NCD122263825_19890622_JFD Electronics - Channel Master_FRBCERCLA SPD_Owner Cleanup 1987 - 1989-OCR

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North Carolina Department of Human Resources
Division of Health Services
P.O. Box 2091 • Raleigh, North Carolina 27602-2091
James G. Martin, Governor
David T Flaherty, Secretary
Ronald H. Levine, M.D., M.P.H.
22 June 1989
Robert W. Speaman
Adams, McCullough and Beard
Attorneys at Law
P.O. Box 389
One Enchange Plaza
Raleigh, NC 27602-0389
Re: Channel Master
NCD 122 263 825
Dear Mr. Speaman:
'Illis letter is in response to your letter of May 1,
1989 concerning lead agency status for the Channel Master
oxford site. It is our belief that a request from the State
at this time for lead agency status would receive a negative
response. It is suggested that this should be a topic for
discussion at the meeting with Channel Master, EPA, and the
State on July 12, 1989. In the meantime, I would like to
assure you that the State of North carolina will continue to
work jointly with the Environmental Protection Agency and
Channel Master Satellite Systems, Inc. to address a
remediation of this site.
'l1lank you for your cooperation. If you have any
questions please contact me at [phone] or Lee Crosby
or Jack Butler at [phone].
™,/JB/db/jack.doc
Sincerely,
aJ~jiY}~
William L. Meyer
Section Chief
Solid Waste Section
State Health Director
/ --
• -
3 February 1989
'IO: File
FRCM: Jack Butler
SUBJECl': Olannel Master, NCD122263825
Mr. John Stelling, Radian Corporation (541-9100) contacted
our office on this date to obtain backgroum infonnation on the
subject site. 'lhis infonnation reportedly was to be used in an
envirorunental audit of a neart>y site that was being sold.
JB/ds/channel. doc:2
• • .J. ALLEN ADAMS
WILLIAM H. MCCULLOUGH
.JOHN Q, BEARD
ADAMS, McCULLOUGH & BEARD
ATTORNEYS AT LAW
E. 0. GASKINS, JR.
. AO BERT W. SPEARMAN
HUGH STE:VENS
CHARLES C. MEEKER
CHARLES rl. MONTGOMERY
CATHARINE BIGGS ARROWOOD
RENEE .J. MONTGOMERY
WILLIAM G. PAPPAS
ALF"REO P. CARLTON, JR
CYNTHIA LEIGH WITTMER
STEPHEN D LOWRY
JOHN F. GRAYBEAL
LISA M. NIEMAN
BLAIR LEVIN
TERRI TOTH Mc KEE
JOHN .J. SUTLER
?OPE MCCORKLE, nt
JAMI:.'.$ K KUYK
HENRY C CAMPEN, JR.
ABRAHAM PENN JONES
JILL B. HICKEY
JIM WADE GOODMAN
OF' COUNSE:L
HEMAN R, CL.ARK
DOUGLAS 0. WICKHAM
P. 0. BOX 389
ONE EXCHANGE PLAZA
RALEIGH, NORTH CAROLINA 27602-0389
TELEPHONE [phone]S64
TELECOPIER [phone]
May 1, 1989
Mr. William L. Meyer, Chief
Solid Waste Management Section
Post Office Box 2091
Raleigh, North Carolina 27602-2091
RE: Channel Master Oxford Site
Dear Bill:
(2iJ
WASHINGTON, D.C. Of'f'ICE
2000 M STREET, N. W.
WASHINGTON, =>.C. 20036-3307
(202) 22.3-0200
NEAL A. .JACKSON
DAVID P. TOWEY
JOSEPH .J. LEVIN, .JR,
JUSTIN A, THORNTON
BARBARA ;:;!OWL.ANO"
LYNN C F1!::LDS
CARL.A CALOBRISI
EDWARD A. BLOOM
DAVID JA:.-!::S WALKERf
OF COUNSEL
PHILIP T. VlrllTE
•MEMBCR CALl~';; .. NIA BA,. ONLY
fMEMBC,. MA.,..,~ND !'A,; ONLY
Our client, Channel Master Satellite Systems, Inc. has authorized us to
request you to seek lead agency status on behalf of the State of North
Carolina from the Environmental Protection Ag·ency with respect to the
Channel Master Oxford site, Recently, Channel ~:laster received a notice
letter from EPA requesting reimbursement of costs incurred by EPA and
beginning the GO-day formal negotiation period. A copy of this letter was
sent to Jack Butler of the Superfund Unit. In light of this action. by EPA,
we believe a request from the State for lead agency status is particularly
important.
Thank you for your consideration.
questions.
Sincerely,
Rl'.'S/rnho
Please call me if you have any
• •
15 May 1989
'ID: File
FRCM: Jack Butler
SUBJECT: Channel Master
Ms. camille Steel, Young, Moore, Henderson, and Alvis,
(782-6860) contacted our office on this elate to obtain backgrourrl
infonnation on the subject site. 'Ihis infonnation is bein;J
gathered for an environmental assessment for Granville Imustrial
Developers.
JB/ds/channel.doc/p.6
~J-Channel • ENCLOSURE 1
rQ. Master~ DIVISION OF AVNET, INC. • '
• P.O. BOX1416 • INDUSTRIALPf\RKDRIVE,SMITHFIELD,N.C. 27577
October 5, 1988
M1·. Jack Butler
Environmental Engineer
Superfund Branch
NC Dept of Human Resources
P. D. Box 209 1
Raleigh, NC 27602-2091
Dear Mr. Butler:
As I noted in our phone conversation on October 4, 1988, Channel
Master would like to backfill a portion of the VOC excavated
area. This is necessary to allow Hamilton Avnet, who is now
moving into two-thirds of the building, access for installation
of several dock doors. It will require approximately 500 cubic
yards of soil to backfill this area. We plan to utilize a
mixture of processed soil and 6ffsite fill dirt to obtain optimum
compaction.
I have enclosed the following information to be submitted to Mr.
Mark A. McClanahan, Ph.D. with the Agency for Toxic Substances
and Disease Registry for his review and comments:
1 . laboratory results for 8
the VOC excavation area
bottom samples)
soil samples collected from
(6 side wall samples and 2
2. a sample location drawing for the above 8 soil samples,
3.
4.
laboratory results
processed soils, and
laboratory results
offsite fill dirt.
for 4 soil samples collected from
for a soil sample collected f,-om
If you have any questions or need additional information please
contact me at [phone].
Very truly yours,
CHANNEL MASTER
Division of Avnet, Inc.
Roger L. Coats
Safety/Environmental Engineer
RLC/sc
cc: Lisa Palumbo, Esq.
Robert Spearman, Esq.
Charles Hansen
Dixie Laswell, Esq.
Joseph Friedman, Esq.
Buddy Mills
AN INDUSTRY LEADER SINCE 1949 • TELEPHONE {919) 934-9711 • FAX [phone]
• •
North Carolina Department of Human Resources
Division of Health Services
P.O. Box 2091 • Raleigh, North Carolina 27602-2091
James G. Martin, Governor
David T. Flaherty, Secretary
Ronald H. Levine, M.D., M.P.H.
10 November 1988
Mr. Roger L. Coats, Safety/Environmental Engineer
Channel Master
Post Office Box 1416
Industrial Park Drive
Smithfield, NC 27577
Dear Mr. Coats:
SUBJECT: Channel Master, NCD122263825
State Health Director
As we discussed on the telephone, your letter and
enclosures of October 5, 1988 addressing the voe excavation on
the subject site (Enclosure 1) was forwarded with my letter of
October 12, 1988 (Enclosure 2) to Dr. Mark Mcclanahan, Agency
for Toxic Substances and Disease·Registry. Dr. McClanahan's
response dated November 4, 1988 (Enclosure 3) is forwarded to
you with this letter for your information.
If you have any questions or comments, please contact me at
( 919) 733-2801.
JB/ds/ibm.51
Enclosures
Jack Randel Butler, Environmental Engineer
Superfund Branch
Solid Waste Management Section
• ENCLOSURE 2 • -:;.,STA'f,
. :,,i; 1
~1 i ""'-,.-~"
North Carolina Department of Human Resources
Division of Health Services
P.O. Box 2091 • Raleigh, North Carolina 27602-2091
James G. Martin, Governor
David T. Flaherty, Secretary October 12, 1988 Ronald H. Levine, M.D., M.P.H.
Dr, Mark Mcclanahan
Agency for Toxic Substances and Disease Registry
Building 30-S Chamblee
1600 Clifton Road, N.E.
Atlanta, Georgia 30333
Dear Dr. Mcclanahan:
RE: Channel Master NCD122263825
Industrial Drive
Oxford, NC 27565
State Health Director
Enclosed please find the letter and laboratory data
submitted to our office by Mr. Roger Coats, Channel Master, on
October 5, 1988, as we discussed in our telephone conversation on
:.Sc:tobe:r 12, 1983.
You will note that this data indicates maximum levels of
soil contamination in the bottom of the excavated area to be 46
ppm cis-1,2 Dichloropropene. As we discussed in our telephone
conversation on this date, the excavation of soil is down to the
water table. Ground water contamination with halogenated
hydrocarbons has been documented on this site and will be
addressed in future activity. The soil excavated from this area
has been "procCcssed" by passing it through a rotary dryer on
site. The maximum contamination in this processed soil is 68 ppb
2-Chloroethylvinyl ether, 20 ppb Methylene chloride, and 16 ppb
Trichlorofluoromethane. Channel Master desires to use this
"processed" soil and off-site fill dirt to refill the excavated
area.
Your comments on this data and planned filling of the
excavated area are appreciated. If you have any questions or
need additional information, please contact me at [phone].
JB/ds/ibm. 28
Sincerely,
Jack Butler, Environmental Engineer
Superfund Branch
Solid Waste Management Section
ENCLOSURE 3
DEPARTMENT OF HEAL. HUMAN SERVICES
Mr. Jack Butler, Environmental Engineer
Superfund Branch
Solid Waste Management Section
Department of Human Resources
Division of Health Services
Raleigh, North Carolina 27602-2091
Dear Mr. Butler:
• Public Health Service
Agency for Toxic Substances
and Disease Registry
Atlanta GA 30333
November 4, 1988
Thank you for the information provided in your October 12, 1988 letter
regarding·the Channel Master Site. You provided a sample location map and
results from 13 soil samples (8 from the excavation, 4 from the excavated
soil, and 1 from the clean fill soil). The chemicals (with their maximum
concentration) reported in the soil samples from the excavation are:
toluene (11 ug/kg), benzene (1 ug/kg), xylenes (2 ug/kg),
1,1,1-trichloroethane (1 ug/kg), trans-1,2-dichloroethene (3 ug/kg),
trichloroethene (46 ug/kg), and tetrachloroethene (19 ug/kg).
Channel Master used a rotary dryer to clean the excavated soil. The
chemical analysis for 4 samples of this cleaned soil showed: toluene (2
ug/kg), 1,3-dichlorobenzene (2 ug/kg), 1,4-dichlorobenzene (2 ug/kg),
methylene chloride (20 ug/kg), trichlorofluoromethane (16 ug/kg),
trichloroethene (4 ug/kg), benzene (2 ug/kg), 2-chloroethylvinyl ether (68
ug/kg), and tetrachloroethene (1 ug/kg). There was no QA/QC information
with the data. The quantitation limit for the 36 volatile organic
chemicals (VOC's) for the contaminated soil was 1 ug/kg. There were no
VOC's found in the sample of the clean fill dirt. For this sample the
quantitation limit ranged from 5 to 10 ug/kg.
The basis of our evaluation and recommendations for this site assumes that
this data correctly represent the level of contamination for the soil
exposed by the excavation, the cleaned, excavated soil, and the clean fill
dirt. Based upon this data further remediation of this portion of the
site is unnecessary. The low level of contamination in the cleaned soil
are insignificant and do not prevent its use to fill the excavation. The
results from the clean fill dirt shows that it _is also acceptable to use
for this purpose. Restoring the area to the original grade with either
the cleaned soil and the clean dirt fill will protect public health.
• •
Page 2 -Mr. Jack Butler
This remediation will stop additional groundwater contamination. However,
the previously reported presence of unacceptable levels of both
trichloroethene and tetrachloroethene in the groundwater requires
cleanup. If you need any assistance with the future activity directed at
remediating the groundwater, I will be happy to help.
Sincerely,
Mark A. McGlanahan, Ph.D.
Toxicologist
cc:
Casimer Pietrosewicz
• DEPARTMENT OF HEALTH & HUMAN SERVICES
Mr. Jack Butler, Environmental Engineer
Superfund Branch
Solid Waste Management Section
Department of Human Resources
Division of Health Services
Raleigh, North Carolina 27602-2091
Dear Mr. Butler:
• Public Health Service
Agency for Toxic Substances
and Disease Registry
Atlanta GA 30333
November 4, 1988
Thank you for the information provided in your October 12, 1988 letter
regarding the Channel Master Site. You provided a sample location map and
results from 13 soil samples (8 from the excavation, 4 from the excavated
soil, and 1 from the clean fill soil). The chemicals (with their maximum
concentration) reported in the soil samples from the excavation are:
toluene (11 ug/kg), benzene (1 ug/kg), xylenes (2 ug/kg),
1,1,1-trichloroethane (1 ug/kg), trans-1,2-dichloroethene (3 ug/kg),
trichloroethene (46 ug/kg), and tetrachloroethene (19 ug/kg).
Channel Master used a_ rotary dryer to clean the excavated soil. The
chemical analys i_s for 4 samples of this cleaned soil showed: toluene ( 2
ug/kg), 1,3-dichlorobenzene (2 ug/kg), 1,4-dichlorobenzene (2 ug/kg),
methylene chloride (20 ug/kg), trichlorofluoromethane (16 ug/kg),
trichloroethene (4 ug/kg), benzene (2 ug/kg), 2-chloroethylvinyl ether (68
ug/kg), and tetrachloroethene (1 ug/kg). There was no QA/QC information
with the data. The quantitation limit for the 36 volatile organic
chemicals (VOC's) for the contaminated soil was 1 ug/kg. There were no
VOC's found in the sample of the clean fill dirt. For this sample the
quantitation limit ranged from 5 to 10 ug/kg.
The basis of our evaluation and recommendations for this site assumes that
this data correctly represent the level of contamination for the soil
exposed by the excavation, the cleaned, excavated soil, and the clean fill
dirt. Based upon this data further remediation of this portion of the
site is unnecessary. The low level of contamination in the cleaned soil
are insignificant and do not prevent its use to fill the excavation. The
results from the clean fill dirt shows that it is also acceptable to use
for this purpose. Restoring the area to the original grade with either
the cleaned soil and the clean dirt fill will protect public health.
• •
Page 2 -Mr. Jack Butler
This remediation will stop additional groundwater contamination. However,
the previously reported presence of unacceptable levels of both
trichloroethene and tetrachloroethene in the groundwater requires
cleanup. If you need any assistance with the future activity directed at
remediating the groundwater, I will be happy to help.
cc:
Casimer Pietrosewicz
Sincerely,
Mark A. McClanahan, Ph.D.
Toxicologist
C. l1cpartrni;nt~o(Human Resources
·isio,, of Health Sct-vicco
State Labomory of Public Health
P. 0. Box 26047
306 N. Wilmington Street
Raleigh. 27611
Time _q.;.__-....:.1.::;;)._...,
::nvironmental Concentrate Comments
__ Groundwater ( 1)
-·_.Surface Water (2)
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
I· J
. . '
C..DIMOO.Stfe,
~ Soil (3)
__ Other (4)
Extractables
Parameter Results mg/1
t/ A . -<o,o I 17" r"'.'ruc 0,05 Zcanum
Cadmium · < 0.0'.3
~hrornium < 0,2,0
( /,llO
§ff;~--< O,Di;,
<D,t:!t,'5_
ver <a· 2,Q
Parameter Results mg/1
-. _ P& T:GC/MS
_ Acid:B/N Ext.
_TOX
MICROBIOLOGY
Parameter
__ (MF) Coliform Colonies/lOOmls
__ (MPN) Coliform Colonies/lOOmls
INORGANIC CHEMISTRY
Total
Parameter Results mg/1 Parameter Resulumg/1
__iL Arsenic <ti-CrJ I/ Silver <IA"
---"::'Bari um ' (
__ Sulfates
__lcCadmium -< +-, i.f __ Zinc
~hloride _Ph
qb __ Conductivity __ Chromium
__ Copper _ms
__ fluoride _TOC
__ Iron
v'Lead ~I{_
__ Manganese
..LMercury < Q, l±.
__ Nitrate.
.JLSelenium < o, l/ ~
ORGANIC CHEMISTRY
Parameter Results mg/1 Parameter Results ing/1
_EDB __ Methoxychlor
__ PCB's __ Toxaphene
__ Petroleum _2,4-D
_Endrin __ 2,4,5-TP C•ilvex)
__ Llndane
RADIOCHEMISTRY
Pan.mete,; Results PCi/1
__ Gross Alpha
__ Gross Beta
)ate Rccdved ________________ _ Date Rcporred ---:---------------
)at< Extracted --------------'----Date Analr.ed ----:-,,-,~;-~-:::-:--::-:::-------
'~; l :) I ? I JUf~ JO 08
:: eportcd By _________________ Lab Number ----------,-----c-----'--
)HS 3101 (R,--,~d 7185)
•.. 1. 1 --.1 u.-~.,4,..,..,., Wsur (Review 7/87)
I
C, ·ccpartmC:nt of Human .Resources
vision of Health Services
A· Sv'?E'RF\ArvD
. ~AMPLE ANALYSES REQ~
State Laboratory of Public He>lth
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611
Timc_q_-_l_;).._-:
'pc of Sample:
Environmental
__ Groundwater (1)
~-· Surface Water (2)
V Soil (3)
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
qvaclrqnf
INORGANIC CHEMISTRY
Extractablca
Parameter Resulu mg/1 Pua.meter Resulu =g/1
<;;:,Ar~nic 5,Q.Ql _i,(Arsenic ( l>,:( 2
7canum 0,Q'i. ~rium ~~-1 · Cadmium · < D, 0 'o ~dmium
~hrornium < D-~o 7rhloride <too I~?-._
~~--
__ Chromium
:s:a,122. __ Copper
<O,QQ2 __ Fluoride
Iver < O-;J.o __ Iron
VLcad '.23
__ Manganese
-lLMcrcury ~ o. l
__ Nitrate.
--l.::'.'.'.'Sc!enium ~0-~(;,
ORGANIC CHEMISTRY
Parameter Resulu mg/1 Parameter Rcaulu =g/1
-.-P& T:GC/MS _EDB
_ Acid:B/N Ext. __ PCB's
_TOX __ Petroleum
_Endrin
__ Llndane
MICROBIOLOGY
Parameter Paramete,;
__ (MF) Coliform Colonics/lOOmls __ Gross Alpha
__ (MPN) Coliform Colonics/lOOmls __ Gross Beta
Commenu
i COM/)Osi'fe
'
Total
Parameter Rcaulu =g/1
Vsilvcr < I.V
__ Sulfates
__ Zinc
_Ph
__ Conductivity
_TD$
_TQC
Pua.meter Rcaulumg/1
__ Mcthoxychlor
__ Toxaphcnc
__ 2,4-D
__ 2,4.S-11' C•ilvcx)
RADIOCHEMISTRY
Rcaulu PCi/1
)ate Received _________________ Date Reported---;--------------
-~•ported By
Jatc Extracted Date Analy::ed ---:-c,,~:,--::-;-:-;-;:~;;--::;-------
v I J I 2U JUi~ J[j 08
_________________ Lab Number ----------,-----------'--
:>HS 3101 (Re\·is.ed 7185)
... 1. l ___ 1 u •••• -4..,..,~ w .. .., .. !Review 7/87)
I
C. beparrmeni of Human Resourc·es
vb.'iotl of Hnlth Services
· -2> v 'f 1::: R F\A N V
_.AMPLE ANALYSES REQ~
St.ate Laboratory of Public Halth
P. 0. Box 28047
306 N, Wilmington Street
Raleigh, 27611
-3q_Q(d.,;i_ac;3o;;i_r-,--::;,Oo-/
ce Number --'-<-__:::c_ _____ .:_:_0 _:::v _____ Field Sample Num\= __ ·--==:: ...J....::::...:c-+---;-----:-------
ame of .Sire __ --..;(,,:::..__· t,,:....._;"_n_n_e-;..:../ :.:..M;__Q;__:,:.S..cl-...:?_-r:__·_-_-____ ~·: ·:Site Location ----;->0""-""'A.i;-'---f'.-'-o'-'-c-"'d'---_______ _
~n~~~d By 5. A .j. ~ {) 0 c[ IDl/ _t.;.J..=5'----Date Colleaed -~G~/ .... 13L.:oC..,/<-"'-g--'rf"----Time 9 -Id--r i ------'=--=
fpe of Sample:
Environmental
__ Groundwater (1)
~--Surface Water (2)
✓ Soil (3)
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
--Othc:r (8)
INORGANIC CHEMISTRY
Extractable&
Parameter Rcsulumg/1 Parameter Re&ults mg/1
""';;,Ar5:"nic <o.ol .-LArsenic < n 99
0.0'7 ~rium KJ Zcanum
· Cadmium · · < O, c,'i$ ~dmium <?-/1.
~hromium < O,';),o ~hloride < /. 60 !CJ jff~_ __ Chromium
<0.02,. __ Copper
-<. '•·' o,a~S: __ Fluoride
. Iver ~0-~D __ lron
v Lead (c ':/.
__ Manganese
___iL'Mercury -<: otl
__ Nitrate
X Scleni.,;,, < Q,S-
ORGANIC CHEMISTRY
Parameter Re&ulu mg/1 Parameter Re&ulu mg/1
-.-P& T:GC/MS _EDB
_ Acid:B/N Ext. __ PCB's
_TOX __ Petroleum
__ Endrin
__ Llndane
MICROBIOLOGY
Parameter Parametct;
__ (MF) Coliform Colonics/lOOmls __ Gross Alpha
__ (MPN) Coliform Colonics/lOOmls __ Gross Beta
Comment>
' (,01>1 /l os, fe_
I
Total
Parameter Results mg/1
I/ Silver < 'J.f\
__ sulfates
__ Zinc
-Ph
__ Conductivity
_ms
_TOC
Parameter Reaulumg/1
__ Mcthoxychlor
__ Toxaphene
--2,4-D
__ 2,4,5-TP (silvcx)
RADIOCHEMISTRY
Re&ulu PCi/ 1
)arc Received _________________ Date Reported---;---------------
)at< Exrracced -------------~---Dace Analy:cd --:--c-,--,-n~~,;-::7,:,--------
'--' i J f c:,--' JUf130 08
.~eporced By _________________ Lab Number ----------,-------~-
)HS 3101 (Rn-iK:d 7185)
... ,. 1 ___ i \.J~-... ,-\r.,,~ Wao~ lRevic...., 7187)
\
C. Dcpa1'tmcni:' of Human Resources
w'isiori of Health Services
. · ~ V 'r i:::. 'RF lJ\ N V
.AMPLE ANALYSES REQ~
Sute l.abontory of Public Hetlth
P. 0. Box 28047
306 N • Wilmington Street
Raleigh, 27611
·3 Cj _Q (-;,_ .;l. a G 3 O;;i_ ,..-5 0 d-~
:e Number --'"----'C:....-----o:;__-=."-----Field Sample Number--------;----,-------
mc of Site __ .__;· G=-· ;_"'...c"'_11_11_e,;_...c/ "-""'-Q'-"-S-'t-'~---r,___-_· ____ ~·: ·,site Location ----;-'0="-_A.,,,_.,_f'....,o....._c_,_c ... J_. --------
,lle~~d By 5 · A .j. uj" O o J ID# _L;-'--""5'----Date Colleacd _....,0C--1-/_,·,..,_3.::.o-1-/-'({"'-"'t'----Time _C/.:.._-...:.1..::::d--:...:........:
·pc of Sample:
Environmental Concentrate Comments
__ Groundwater ( l}
__,__· Surface Water (2)
__ Solid (5)
__ Liquid (6)
· Cj uad // Com ops I le__
. I
I/ /?
V 'Oil (3)
__ Other (4)
__ Sludge (7)
__ Other (8)
Extractablcs
Parameter
Parameter
-.-P& T:GC/MS
_ Acid:B/N Ext.
_TOX
Para.meter
Results mg/1
<c.01
Do5
<o.(13
( 0, :/,0
</.OD
< o. ;,,o
Results mg/1
MlCROBlOLOGY
__ (MF) Coliform Colonics/lOOmls
__ (MPN) Coliform Colonics/lOOmls
INORGANIC CHEMISTRY
Parameter
_L Arsenic
~rium
~drnium
-Chloride
_../_ r Chromium
__ Copper
__ Fluoride
__ Iron
~Lead
__ Manganese
---1<::Mercury
__ Nitrate.
_!L:sc!enium
Results mg/1
<o.o9
ORGANIC CHEMISTRY
Parameter.
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ Llnd.ane
Results mg/1
Pan.mete,;
--Gross Alpha
__ Gross Beta
Total
Parameter
Vsi\ver
__ sulfates
__ Zinc
_Ph
__ Conductivity
_ms
_TOC
Parameter
__ Mcthoxychlor
__ Toxaphcne
-2,4-D
Rcaulumg/1
Rcaulumg/1
__ 2,4,5-11' (silvcx) _____ _
RADIOCHEMISTRY
Results PCi/1
)ate Rccdv,;d ________________ _ Date Reported---:--------------
C:eporred By
)ate Exrracted -------------~---Date Analy-..cd ---:-;-:,-,,-~;;-;;-~c"r'?T'"------u 1 ..) : ;. ..) _iurj :rn Ee
_________________ Lab Number ---------...,.....----,--......;._
)HS 3\01 (Rc-~·i!,Cd 7185)
..• t. J ---' u •. ~,,-ln.,~ Wa..re (Rcvic..,.• 7187)
i
C.~Dep_ar~cnt o{ Human ·Resources
•isiori' 9( Hc:1lth Services
· ~ v f 1:::. 'R flA (I) V
.MPLE ANALYSES REQ~
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
lWcigh, 27611
·3 q .Q I ?. ;;i_ a ~ 3 o-, ,----;:, 0 -, ~
e Number ~--------0_'7'-_u _____ Field Sample Numbcr __ 0_· --=---:-..J~-,-,.------
mc of .Site ·. (.., I,. " 11 n e.-/ IV\ Q .S f i>-r . -. ·:::Site Lociition ----:-· 7 Q=--'A.'y-~f~o~c ... J.._. _______ _
llectcd By 5. A + ,;j' DO J ID# _4~5 __ Date Collcaed --"(;'--+/ .... 3'-'0'-,l-/-"'({'-'6"-----Tunc _9_-_I d-_ _,
pc of Sample:
::nvironmeno.l Concentrate Coromenu
__ Groundwater ( 1)
-· _· Surface Water (2)
~ Soil (3)
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
--r (} F J,_,, en t:
__ Other (4)
INORGANIC CHEMISTRY
Extractable,; Total
Parameter Results mg/1 Parameter Rc,;ulu mg/1 Parameter Resulumg/1
~Ar"'.'nic :s:_o. o I -LArscnic 0,'-f.s Vsilver ( /Cf
~anum
0, /I) ~ rium f<t_ __ Sulfates
Cadmium · · < o.o'ii ~dmium {. +, i, __ Zinc
~hromium <D. 2iD :7f:hloride _Ph
<. /. DD c.(.] __ Conductivity
IF~-__ Chromium
sa,62:; __ Copper _TDS
< 0. o.b.'s. __ Fluoride _TOC
vcr <c,-~D __ Iron
VLead L,?i.~
--Manganese
~Mercury Q, l
__ Nitrate.
..J.LSclenium ~ o.q_r
ORGANIC CHEMISTRY
.Parameter Re&ulumg;/1 Parameter Rc,;ulu mg/ 1 Parameter Results mg/1
-. _ P& T:GC/MS _EOB __ Mcthoxychlor
_ Acid:B/N Ext. __ PCB's __ Toxaphcne
_TOX __ Petroleum _2,4-D
__ Endrin __ 2,4,5-TP (,ilvcx)
__ Lindanc
MICROBIOLOGY RADIOCHEMISTRY
Para.meter Para.mete,; Results PCi/1
__ (MF) Coliform Colonics/lOOrnls __ Gross Alpha
__ (MPN) Coliform Colonics/lOOmls __ Gross Beta
)a<e Receivc;d _________________ Date Reported---:---------------
"..cporred By
)ate Exrracted -------------~---,-Date Aruly-.<:d ----:-:--.,-,-~,--;;--;:-~-:--;,c-=------
.J i JI/\ ,iUf,3038
_________________ Lab Number ----------,-----,---..c_
)HS 3101 I Rc\·is.cd 7185}
-.1. I --.1 U,.-..,..4,..,.,.~ WaoC"" (Re-vie""'' 7187)
I
... • I,,,. ..,1.:.,L, l'U\..LJ."J...::;.J.\ .L vr OUI".l.fiJ., I\.L.:tVUl\.l.,,t.,,)
---~IVISION OF HEALTtl SERVICES
SOL-wu'IJ HAZARDOUS 1,/ASTE MANAGFW:'•-~.ANCR
Chain of Custodv Record
Hazardous Waste Materials
Location of Sampling: Generator __ Transporter _Treatment Facili
__ Storage Facility __ Disposal Facility __ Landfill
✓ Other : ___ O;_w:.::..;".:..::e..:.:r _ __,c,__,l.se.'"A-'-'-'-'f\'-'°'"'-l=f"-------------
Company's Name LhA,...Y\e_\ MA~ i<=--~ Telephone( ____ ) _______ _
Address Qy:_, '\-a rd_ f-) c__
Collector's Name. __________________ Tele_phone( ____ ~) ________ _
signature
Date Sampled;.___.;:;G......,;3::;._o ____________ T.ime Sampled;..__9_,__---:.../.;..;2..~.' 0;;;...;;o __ _
Type of Process Generating Waste ·------------------------V
. Field Infonnation
· ·:Field Sample No. 3 0 I 4
1.
, (} <-I title inclusive dates
2. ~ or-m-J
3. lit;~~ title inclusive dates
signature = inclusive dates
~124~
signature title
Instructions: Complete all applicable infonnatic,n including signatures, and
submit ~ith"Bnalysis request for.:s.
!..IJ. \' J...:>J.Ui\ U.r .t..tfU..,Lt:1 St.KV·lC.tS
SOLID AND HAZARDOUS wASTE MANAGEMENT 41/J<CR
.eceip: for Samples
The samples described belm, were collec.ted in connection with the administration,
enforcement, and documentation of the:
( ) North Carolina Hazardous Waste Management Rules, 10 NCAC lOF
() North Carolina Solid Waste Management Rules, 10 NCAC lOG
( ) Comprehensive Environmental Response, Compensation and Liability Act: '(CERC-i..A)
() Toxic S~bstances Control Act: (TSCA). 15 U.S.C. s2601, ~ seq., specifica1ly
Section 11 . of TSCA, 15 U.S. C. Ii 2610.
Inspector_' s Name
Name of Fi=
Cl'lfl n i'1 ,e,../ · M ,~-u f-e_;-
Fim Cr.mer,
//'
{{Aho ,,_....
Ope~·a ::or; or Agent
d. l ~ _+r, -
SAMPLi COLLECTED SAMPLE TYPE
l,7.JMBER DATE TIME WATER SOIL.
I b(3D q.1-zN1
2 I \ I
3 I
~ I l
5 J -I
'
.
I
Receipt for the sample(s) described.
aoove is hereby acknowledged:
~ at;;;;;;JJ
Signature of Inspector
Tii:le
O'I".:iER
Inspector's Address
Firm Address
Title
_<; o-,{e:l-y 'Jin v, 'rouV'A£ui--,,) ;:::;:. . ' 1--1,4 ,1 ,,..,,e,-e,r .
'/ ,, /2
DUPLICATE SAMPLES SAKPLE LOCATION
OITEREDIACCEPIED REJECTED •ON-SITE OFF-SITE
-. ..
✓ I J \JVQJ...\.. Go, ~o,.;~._ ( O~:,") n11, s"'""" J,-10 (o''3")
. ./ I / q ,U<Ad 'J: C.o 'l'fo,, I,: (\'Z"~
. l:.icl\ So."'(\< s (o-10 (\2"\
/ _/ 0-~~, '1t c..,, ~f,.;l:e Ul'-1,"\
1:.'c~, S.Ol,r(},,s 1-5(.o"-n
../ _./ Gl. '-'°'6 JI. c.__ I 1/<'~osi\t_~\
I.I'./\ s"'""~' C \ .c:. ( 1'2."'\
✓ / 'Il'\~\1ieJ . -" .. ~ ..
(I\:, ~,.,.,I. II\
i
'
I
Receipt/rejection of duplicate or split
samples is hereby acknmdedged·:
~p\/ -:;L: (a.?,/4_ --
Signature of Finn Owner, Operator, __ or Agent
Title 'C · {,/
COM!-fENTS ·-------------------------------
I"'~ Channel • • ,, ... Master® D1v1s10N oF AVNET. 1Nc • P 0. BOX 1416 • INDUSTRIAL PARK DRIVE, SMITHFIELD, N.C. 27577
De tober 5, 1988
Mr. Jack Butler
Environmental Engineer
Superfund Branch
NC Dept of Human Resources
P. 0. Box 2091
Raleigh, NC 27602-2091
Dear Mr. Butler:
As I noted in our phone conversation on October 4, 1988, Channel
Master would like to backfill a portion of the VOC excavated
area. This is necessary to allow Hamilton Avnet, who is now
moving into two-thirds of the building, access for installation
of several dock doors. It will require approximately 500 cubic
yards of soil to backfill this area. We plan to utilize a
mixture of processed soil and offsite fill dirt to obtain optimum
compaction.
I have enclosed the following information to be submitted to Mr.
Mark A. McClanahan, Ph.D. with the Agency for Toxic Substances
and Disease Registry for his review and comments:
1. laboratory results for 8
the VOC excavation area
bottom samples)
soil samples collected from
(6 side wall samples and 2
2. a sample location drawing for the above 8 soil samples,
3. laboratory results for 4
processed soils, and
soil samples collected from
4. laboratory results
offsite fill dirt.
for a soil sample collected from
If you have any questions or need additional information please
contact me at [phone].
Very truly yours,
CHANNEL MASTER
Division of Avnet, Inc.
Roger L. Coats
Safety/Environmental Engineer
RLC/sc
cc: Lisa Palumbo, Esq.
Robert Spearman, Esq.
Charles Hansen
Dixie Laswell, Esq.
Joseph Friedman, Esq.
Buddy Mills
AN INDUSTRY LEADER SINCE 1949 • TELEPHONE [phone] • FAX [phone]
• •
4 May 1988
TO: Bill Meyer, Olief
Solid Waste Management Section
FRCM: Lee Crosby, Head
SUperfund Branch
RE: Channel Master
1) Pat DeRosa has located the OJV<;;!:; procedures for laborato:ry and
field work (memo from Pat is attached) . We have a copy of the
field manual, but not of the laborato:ry manual. Channel
Master nay obtain one copy of each free. Would you like for
us to copy the field manual for them or just send a letter
telling them where to order the infonnation? (A letter to
Dixie Laswell is attached for your signature.)
2) The letter was received in April 1988. A copy is attached for
your convenience.
3) Jack &!tier has talked with the town engineer and feels that a
meeting is needed with you, Olannel Master, DEM, and Oxford
city officials, including the city engineer. We can schedule a
meeting for you, if you think this is appropriate.
4) Jack has also written to COC to ask for a determination of a
cleanup standard for rretals at Olannel Master. His letter is
also attached. We expect a response in approximately one
month.
LC/tb/73
• •
29 April 1988
TO: File
FRCM: Jack Butler
RE: Telepmne amversation with Mr. Denise Ramsey, NRCD Assistant Section
Chief for Envirornrental Operations, Water Quality Section (733-5083),
about Channel Master, N::Dl22263825.
As requested by Mr. Chuck Wakild on 28 April 1988, Mr. Denise Ramsey
was contacted on this date to discuss the subject site. Mr. Ramsey reiterated
that any discharge to the ditch \\Ould require a NPDES permit with Water
Quality Standards as the discharge limits. These limits \\OUld include 0.050
mg/1 chromit.ml and a toxicity test for the chlorinated hydrocarbons.
Mr. Ramsey stated that if a rreeting is held beo-.een our office, the
Town of Oxford, Channel Master, and NRCD that either he or a representative
from the Raleigh field office smuld be included.
JB/pb/0576b.28
• •
28 April 1988
TO: File
FRCN: Jack Butler
RE: Telephme conversation with Mr. Chuck Wakild, NRCD Water Quality
Section Chief (733-5083), al:out Channel Master, NCD122263825.
Mr. Wakild was contacted on this date to discuss water discharge
options and NPDES permit requirellY2nts and procedures for the Channel Master
site in Oxford, N .C. Mr. Wakild reported that if the ditch to be discharged
to is essentially a dry ditch then the water discharged to it \>Ould be
required to 11Y=et water quality standards. Mr. Wakild alro infor11Y=d re that
1:x:ith of Oxfords t\>O waste water treatment plants ~re having trouble reeting
the limits of their present NPDES permits. This has resulted in a moritoriurn
on expanding their collection system. Mr. Wakild added that I might also talk
to Mr. Denise Ramsey, Assistant Section Chief for Erwironmental Operations for
NRCD.
JB/pb/0576.32
• •
28 April 1988
TO: Lee Crosby
FRCM: Jack Butler
RE: Charlffil Master, OCD 122263825
On April 25 through 28, 1988, I cxmtacted Mr. H. Tom Ragland, Oxfurd
Town Manager, Mr. C.D. Malone, Hydro Management (Oxfurd Town Engineer); and
Mr. Dale Overcash, and Mr. Chuck Wakild, NRCD Water Quality Section,
concerning tre subject site. During these discussions several issues .ere
identified related to discharge of water from the lagoon (short term) and from
an extraction .ell (long term) to the city se.er or the ditch adjacent to tm
site.
1. Oxfurd representatives would like to know if the Town of Oxfurd
could be provided any assurance that trey 1-.0uld rot be cited, if
accepting water from the Channel Master site resulted in the town
violating their NPDES permit. Mr. Chuck Wakild, NRCD Water
Quality Section Chief, pointed out that the Town of Oxfurd at
present has two waste water treatment plants, l:oth of which are
having trouble meeting their present NPDES permits. This has
resulted in a monitorium on expansion of the Oxfurd waste water
collection systems.
2. Mr. Tom Ragland, Oxfurd Town Manager, pointed out that Channel
Master has rot been charged fur any discharges from tre lagoon
during the cleanup. Mr. Ragland feels that any long term
discharge plan (ie. extraction .ell) would require payment of
some kind from Channel Master for se.er use.
3. Any discharge to the ditch at the edge of the property would
require a NPDES permit. The permitting procedure takes
approximately 4 to 6 months.
4. Since the flow in the ditch 1-.0uld be essentially 100% from the
Channel Master site (tm ditch is presently dry), the water
discharged to this ditch would be required to meet water quality
standards.
It is reconmmded that a meeting be held bet.een IER/IRS Solid Waste
Section, NRCD Water Quality Section, the Town of Oxfurd, and Channel Master.
All parties contacted appeared to feel that such a neeting would be beneficial
to help each group understand the position and concerns of the otrer groups.
Lee Crosby
Page 2
• •
Dr. Mark A. McClanahan, U.S. Agency for Toxic Substances and Disease
Registry (ATSIR), was contacted on 25 April 1988 to discuss the Channel Master
site and a reIIY2diation level for chromium in the soil at this site. Dr.
McClanahan reported that their experience across the U.S. indicated that
chromium occurs naturally in soil at concentrations of from 5 to 3,000 pµn
with a median of 100 ppm. They have also determined in general that from 5 to
200 ppm total chromium in surface soil is acceptable for residential use and
that up to 10 times this level is acceptable in surface soil for industrial
use. After discussing the history and data for the Channel Master site Dr.
McClanahan indicated that there should be ro problem in filling in the present
pit with clean fill at this tiIIY2. Dr. McClanahan agreed to respond in writing
upon receipt of a concise package describing the present status of the site.
This package was prepared on April 27, 1988 and will be mailed to Dr.
McClanahan within a day or t:v.U.
JB/pb/0489b.50-51
• •
26 April 1988
TO: File
FR(],!: Jack Butler
RE: Teleph:me conversation with Dale Overcash, NRCD (733-5083) about NPDES
pennits and Channel Master, OCD122263825.
Mr. Overcash was contacted on this date to discuss water discharge
options and NPDES pennit requirerrents and procedures fur the subject site.
Mr. Overcash reported that an NPDES pennit fur the Channel Master site \\Ould
probably take 4 to 6 m:mths to obtain as a minimum. The testing required
\\Ould probably include such things as toxics, chromium ( 50 ppb), oil and
grease, soluble solids, and turbidity. This testing is usually required
quarterly. Mr. Overcash also added that if the discharge ..ere to a ditch with
no present flow (ie. discharge \\Ould be total flow) then there may be a
problem with the Ground Water Section of DEM.
Mr. Overcash was also asked about any assurances that DEM could give
the Town of Oxfurd not to cite them fur NPDES violations that could result
from the town accepting discharges from Channel Master. Mr. Overcash noted
that one problem that he foresaw for any such agreerrent WJuld be in
attributing problems at the town se..er plant to discharges from Channel Master.
Mr. Overcash concluded that any rreetings involving DEM or NPDES policy
decision sh::>uld include Chuck Wakild, Water Quality Section Chief (733-5083):
JB/pb/0576b .31
• •
26 April 1988
TO: File
FRCM: Jack Butler
RE: Telephone a:mversation with Mr. H. Tom Ragland, Oxfurd Town Manager
(919-693-2195) about Channel Master, N:D122263825.
Mr. Ragland was contacted on this date to discuss the subject site and
the termination of the temporary se\ser discharge permit at the end of May
1988. Mr. Ragland expressed concern over the length of this project. It was
explained that some of the delays \sere due to the time involved in sampling
and turn around of lab results. Mr. Ragland also expressed concern over the
fact that the town had mt charged Channel Master fur any of the discharges
over the past year or tw::>. He aloo wanted to avoid a situation where the town
w:iuld be penalized because of discharge accepted from this facility. (The
town had been cited fur violating their NPDES permit due to discharges from
this facility when it was operated by JFD.)
In conclusion Mr. Ragland felt a meeting be~en the town, Channel
Master, DEM, and our department w:iuld be of benefit to all. In particular Mr.
Ragland would like to discuss charges to Channel Master fur se\ser use and
protection from being cited if any discharge from the Channel Master facility
caused the town to violate its NPDES permit.
JB/pb/0576b.25
• •
25 April 1988
TO: File
FRCM: Jack Butler
RE: Telephme oonversation with Dr. Mark A. McClanahan, ATSDR
(404-488-4100), about Channel Master, NCD122263825.
Dr. McClanahan was contacted on this date to discuss the subject site
and a remediation level for chromium. Dr. McClanahan reported that treir
experience across tre U.S. indicated that chromium occurs naturally in soil at
ooncentrations of from 50 to 3,000 ppm with a median of 100 ppm. They have
also determined in general that from 5 to 200 ppm total chromium in surface
soil is acceptable for residential use and that up to 10 times this level is
acceptable in surface soil for industrial use. After discussing the history
and data for the Channel Master site, Dr. McClanahan indicated that there
smuld be no problem in filling in the present pit with clean fill. Dr.
Mcclanahan agreed to respond in writing if I would submit a package stating
tre situation at this site. This package smuld be mail to the following
address:
Dr. Mark McClanahan
Agency for Toxic Substances and Disease Registry
Bldg. 30-S Chamblee
1600 Clifton Rd. , N .E.
Atlanta, GA 30333
JB/pb/0576b.24
• •
25 April 1988
TO: File
FR(},!: Jack Butler
RE: Telepmne conversation with Mr. C.D. Malone, Hydro Management
(l-800-722-0469), about Channel Master, NCD122263825.
Mr. Malone was contacted on this date to discuss the subject site and
termination of the temporary sewer discharge permit at tl~ end of May 1988.
Cleanup activity to date was described to Mr. Malone. Mr. Malone reported
that he had recommended that the water be discharged batchwise through the
m lding tanks on the site to minimize risk to the se..-er plant. Mr. Malone did
mt think that the cut off date of May 30th was absolute but he had some
concerns over an open ended extension, especially considering that Channel
Master had mt discharged any waste water since late December 1987. It was
explained to Mr. Malone that the delays in progress and gaps in discharge ..-ere
due to delays in sampling and return of lab results. Mr. Malone did think a
meeting bet..-een him, the Town of Oxfurd, Channel Master, and our department
could be of some benefit to all.
JB/pb/0576b.26
• •
5 April 1988
TO: File
FRCM: Jack Butler
RE: Telepmoe amversation with Jessica Lau, Law Tech, about the Channel
Master Site, NCD122263825
Ms. Lau rontacted our office on this date to request a ropy of the
Ground Water Evaluation Report dated N:lv. 1986 . I agreed to have this report
ropied and mailed to Law Tech if Ms. Lau ~)Uld request this ropy in writing.
Ms. Lau also in:funned me that Allan Lemir had been assigned to this project
as the attorney :fur EPA Region IV.
JB/pb/0586b.25
TO:
FROM:
SUBJECT:
• •
30 March 1988
File
Jack Butler
Telephone conversation with Roger Coats (919-934-9711) about
Channel Master, NCD122263825
Mr. Coats contacted our office on this date to give an update on the
clean-up activity at the Channel Master site in Oxford. In the next two days
Mr. Coats expects to transport approximately 30 truck loads of material from
the lagoon area which has been stockpiled on the site for several weeks. Mr.
Coats will forward the manifests and a written update on this project next
week. Mr. Coats also reported that Channel Master had received a letter from
the Town of Oxford informing them that the city will not accept any more water
from the lagoon into the city sewer after May 31, 1988. Mr.Coats and I also
discussed briefly how the cities refusal to accept wastewater from this site
will impact the ground water remediation planned at this site.
JB/ds/0572b.44
• •
North Carolina Department of Human Resources
Division of Health Services
P.O. Box 2091 • Raleigh, North Carolina 27602-2091
James G. Martin, Governor
David T. Flaherty, Secretary
Ronald H. Levine, M.D., M.P.H.
Mr. Patrick M. Tabin, Division Director
Waste Managena1t Division
18 Marcil 1988
United States Envirornrental Protection Agency
345 Courtland street, N.E.
Atlanta, Georgia 30365
RE: 01annel Master NCD122263825
Oxford, North carolina
Dear Mr. Tabin:
State Health Director
North carolina is requesting that Channel Master be deferred from listing
on the Upjate #7 proposed National Priority List. Channel Master is in the
process of rerrroial activities and state authority is adequately addressing the
clean up.
Since the date of the Site Investigation and draft HRS submittal, Channel
Master has been engaged in an extensive cleanup project of heavy metal
contaminants in the lagoon area on the site. This initial cleanup is being
conducted urrler the supervision and with the approval of this office and with
the cooperation and kna,;ledge of EPA Region IV. All Channel Master cleanup
plans and sampling results have been submitted to EPA. To date, O!annel Master
has rem:wed approximately 700 loads, at approximately 20 cubic yards per load,
of soil and sludge in the lagoon area to a permitted disposal facility.
Channel Master estimates that this quantity represents approximately 80 percent
of the total quantity of sludge and soil to be removed from the lagoon area at
the site. Channel Master presently is in the final stages of the removal and
disposal of the remaining quantity of this material.
'Ille draft HRS score was well above the 28.5 cut off for NPL consideration
based on 25 February 1987 site conditions. If the site is ranke::l based on
present site conditions, the score is 19.55. Although the current NCP does not
permit cleanup activities to effect the HRS score, we request that a score
based on the cleanup be considered for deferment of listing as long as the
cleanup is in progress. Channel Master has made and continues to make
substantial site remediation progress.
•
Mr. Patrick M. Tobin
18 March 1988
Page 2
•
It is my understarrlin;J that the National Contin:Jency Plan draft
Section 300.102(a) State Involvement in the Listin:J and D=listin:J Process
provides that the state's request to defer listin:J will be reviewed prior to
publication of the proposed listin:J. Again, state authority can adequately
address remediation at Olannel Master. Dc!fennent at this time nay be
corrlitional on Olannel Master pursuing a pemanent remediation of the graurrl
water contamination problem on the site under the continued supervision of and
in cooperation with this office and EPA. If the remedial action plan, the time
schedule, or the clean-up action is found at any time to be unacceptable by the
state of North carolina or U.S. EPA Region rv, the defennent from NPL inclusion
could be re-evaluated.
If additional infonnation is needed to defer listin:J of Cllannel Master,
please contact this office at [phone].
Sincerely,
u),iJL_ ;1 m~
William L. Meyer, Olief
Solid Waste Management Section
WIM/tb/ibm-37
TO:
FROM:
SUBJECT:
• •
17 March 1988
Fi l e
Jack Butler
Telephone conversation with Charles Hanson and Roger Coats,
Channel Master, NCD122263825
Charles Hanson and Roger Coats contacted our office on this date to
discuss the status of the clean up at the Channel Master site in Oxford, NC
and the NPL listing status of this site, Mr. Hanson and Mr.Coats reported
that approximately 30 loads of contaminated soil had been shipped off site in
the last couple of weeks and that they expected to ship an additional 60 or so
loads before the lagoon area would be ready for sampling again. Mr. Coats and
Mr. Hanson agreed to inform our office when they were ready to sample the
lagoon area again so that we could be present for the sampling and to split
samples with Channel Master,
Mr. Coats and Mr. Hanson reported that they had been contacted by
Jessica Lau of Tech Law as part of the PRP study for the Channel Master site.
Mr. Coats and Mr.Hanson expressed concern that this PRP study meant that
update 7 of the NPL had been published. They were informed that to our
knowledge update 7 of the NPL had not been published yet and that EPA Region
IV had informed us that it was expected to be published in late April.
Mr. Hanson also expressed concern that their request to EPA Region IV
for the state to oversee the cleanup of this site had caused them to become an
NPL site. Mr.Hanson was informed that their status as a potential NPL site
was unrelated to our overseeing the clean up activity at this site.
JB/ds/0572b.35
-
S. C. OcpJ.r:mcnt ofHum:i.n Re.sources • -
L',,i,,oa of Hc,l,h Sm,ecs . SAMPLE ANALYSES REQU£!!!1!'
St.ate Laboratory of Public Health
P. 0. Box 28047
306 N. \Vilm.in.gton Srrcct
R.,Jcigh, 276 I I
Site Numbc-r _s/_d)_/_U __ Z_o_3_,F'._2~S'~----Field Sample Number ~3~6:~-~0_0 __________ _
NameofSit< C/2anndcl darfe-v
Collected By So-,l'A'~rM T,,, f,·,tq I.DI/ Z: Z::
-"70, C ,<" dJ"' t I e,.?
J ypc of Sample:
Environmental
__ Groundwater (I)
__ Surface Water (2)
V Soil (3)
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
--Othet (8)
Site !.=ion O d7'.'2, ,,.c,/ . A/, C,, :,
Dare Collcaed ;z;. Vl, 2 ,s;;; I 9'c:£cf' " Time /0 JO
Comments
::r .]
INORGANIC CHEMJSTRY
Extractable, Total :...-··-·-·
Parameter Results mg/1 Parameter Results mg/l<J · Parameter Rcsu! ts =g/ 1 Y:,
...=:::::...Arsenic ~,OJ ✓ Arsenic < (. '1 V Silver <rz o
-' Barium ..L..Barium k fJ. __ Sulfates
../Cadmium . '.~ /( ./Cadmium ~-0 __ Zinc
•'
~Chromium <O-~ __ Chloride _Ph
__ Lead <&~ -'<'.'.'.'..Chromium --:i, /..J. __ Conductivity
VMercury _Copper _ms -
.. ,Z;~k11iu_rn ___ ~ .o ~-__ Fluoride _TQC
-Silver s::::: Q • )._Q __ Iron --
--✓Lead 'J.' ()_ --
_Mangan~ ·.
----
--✓ Mercury < o. I --
--__ Nitr.ue --
--/Sc!eni~ <Q.V --
ORGANIC CHEMISTRY
Parameter Rcoult,mg/1 Para.meter
_P&T:GC/MS _EDB
__ Acid:B/N Ext. __ PCB's
.
_TOX __ Perroleum
--_Endrin
--__ Lindane
MICROBIOLOGY
Parameter
__ (MF) Colifomi Colonies/lOOmls
J __ (MPN) Coliform Colonies/lOOml.s
----
Dare Recc:ivc;d _________________ _
Dare-Extracted--------------~---
Reported By
:l?;S ) IO! ( R<"•·1x.:l / 185)
~1\i..! ~nJ H~:.Jrdous \J,.:Hl< (Rc\'irw i/87)
Rcsulu mg/1 Parameter· Results =g/1
__ Methoicychlor
__ Toxaphene
_2,4-D
_ 2,4,5-TP (sU~cx)
--
RADIOCHEM:ISTRY
Parameter Results PCi/1
__ Gross Alpha
__ Gross Bela
----
-·01/•"·•7 ,co,r,.'"f\ Lab Num bcr _ __,(.,,).,.' __.__ ... r )~-,~~, u: ,~· ,.,_! .Li'..l.iL) .:::'-'c:'.J:....... ______ _
-~-C. Depart:nent of Human Resources
Di,•:ision of Health Services ·
St.ate l...ab..?rato[)' of PubUc Health
. P. 0. Box 28047 • SAMPLE ANALYSES REQU.
306 N. Wilmington Srrecc
!Weigh. 276 I I
Site Number _SJ---'-_d)_/_.z.:l __ 2._C--'-3--'J>'--. _2~S'=--------Field Sample Number ~3"--"-6'~S:_/ ______ ,__ ____ _
Name of Site CA an J1,;;;J I da,t fe v Site L=ion O .-o::2,·..,.a(, -d/,, C> .>
Collected By Soµ1/te.r,-, T c..r f.-,,q ID#.~f-'---'z:: ___ Date CoUcacd tfen, .Z.5; l'l',Pcf' ..
, · Jotc~ dlnt/,e,,:'
Time //00
Type of Sample: ·
Environmental
__ Groundwater (1)
__ Surfa~c Water (2)
V Soil (3)
-.-Other '(4)
C-onccntratc
__ ._ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ ()thcr (8)
INORGANIC CHEMISTRY
· 'Extractable< ,, . · .
Parameter . ·.Results mg/1
-· --'-------'------'----
· , Parameter
· ·· · Manganese :=2' M~curv' . ,
__ · Nitrate .
LSdcniu.:n
Total
-< Io
--.,.------'------.,-------
--.-----,---------
ORGANIC CHEMISTRY·· :.: , .
Parameter .. _. . · Rcsulu.mg/1 · · Par.unct;,,.. .
,. . .
_P&T:GC/MS
__ Acid:B/N Ext.
_TOX.
. · MICROBIOLOGY
; ~an.meter . : ;
__ (MF) Coliform Colonies/lOOmls ·
__ (MPN) CoHform ·colonies/lOOrnls
.
~l!--15 3 IO! ( Rc---1K.:i f /85) ,·/.
;..,,1iJ mJ H~:.Jrdoul \I.:auc (Re_ .... ie, ..... ··i/a7)
_· -EDli·
_· _. _PCB's ··
_·, -·-Petr;,leum
__ Endrin
_. _Lindane ... '
Results mg/1 Par.u:netcr.•,. . R,auiu JJ:W'l .
.. _',_ Mechoxyduo;.
_._, Toxaphc:ne ;. ,:· ,----·----
------'----· __ 2,4-D : ' .•. >· _ ..,.-------
_· ·_. 2,4,5-TP (sil~cx)
-P~etCr• ·
__ Gr;,ss Alpha .
__ Gross &ca
RADIOCHEMISTRY
· Rdiulu PCi/1
•
S. C. Oc;:iartmcnc of Human Re.sources
Div~sion of Health Services .SAMPLE ANALYSES REQU~
St.ate Laboratory of Public Hcal(h
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611
Site Number _s/-'---'-d)_/_2.:l __ Z_o_.3.c.....c,?_2_____,S'=-----Field Sample Number ~]~6~S:~Z-___________ _
NameofSice CAa,,,,11,21 da,rfey
CollemdBy Sov?'/te,y,,, TCJ"f,11<1 ID/I_ lflf
T (s I Jo,c/: ttln tie,::'
ypc o amp c::
Environmental
.---Groundwater (1)
___ Surface Water (2)
V Soil (3)
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
S ice Loca,.-ion O --rz:2, v ef --4-:r C c . 7 .
Date Collected ,:Z:.,. v1, 2 .s;; I 9'c9cf' . · Time // J 0
Comments
INORGANIC CHEMISTRY . .
.
Excractables Total •-w••••••••••
Parameter Results mg/1 Parameter Results mg/lj-· Parameter Results mg/~
J.L.Arsenic < o, Q l V Arsenic < o . .r ,/ Silver· <. I 0
_LBarium (),/() ✓Bari 2'7 _·_·Sulfates --um
__JZ:..c.dmium < ()_. /)_i_ ,.LCadmium 'f_,Q _-_-Zinc
../ Chromium ~~ .. ~~ __ Chloride _Ph
../1.ead ✓ Chromium l'l:.6. __ . Conductivity
v Mercury ~:~rj' __ .Copper _TDS -
✓ Selenium __ Fluoride _TOC :z-·--·----Silver _· _Iron --
--../ Lead 'i., 0 --
----Manganese . --
-·-✓ Mercury < Cl. • z --
--__ Nitrate --
--v' Selenium < {., Q --
.
ORGANIC CHEMISTRY
Parameter Resulcs.mg/1 Parameter Results mg/ 1 Parameter· . Results mg/1,.,
' _·_Methoxychlor '_P&T:GC/MS _EDB
__ Acid:B/N Ext. __ PCB's __ Toxaphene
_TOX __ Petroleum _2,4-D.
--__ Endrin __ 2,4,5-TP (sil;ex)
--_. _· Lindane --
. MICROBIOLOGY RADIOCHEMISTRY
Parameter Parameter R~ulcs PCi/1 ·, ..
__ (MF) Coliform Colonics/lOOmls __ Gross Alpha
__ (MPN) Coliform Colonics/lOOmls __ Gross Beta
----
----
Dare: Rc:cc:ivc;d Date: Rc:poned qtvi~YY
Datt'" Exrractc:d Da« Anal,~..ed
Rep0rced By Lab Number OOlbJ'-/ 1~1:9:~r;3 v,-.,1 Lu·L·.
~)~5 31 o ! ( RC'\"I~..-::! 7185}
:>..,Ii.I mJ H.i: .. u.:!ous \lhm: (Review 'i/87)
-
.:,./ C. Dcpanmc;:it or" Humm Rc.sourc:s
'Di."ision of Health Scn"lces • SAMPLE ANALYSES REQU.
S~tc Liboratory of PubLlc Holch
P. 0. Box 28047
306 N. Wilmington Sue-cc
Raleigh, 276 I l
sire Number .3'1dJ/2-Z:Z.0 3? 2 .S-Field Sample Number ~J_b~S_3_~---------
Name of Si;, CA an t/d I da.r fey Site J.,oca,."ion Od'.Z'1).viacS A/'rQ~
Collected By So,,?/te.r,-, T CJ' T,·11q IDll.-ff-'-"'----Date Collecte~ CJo ._;, .Z,s_;; I 'Tcf>cf' ..
T . rs· I Jo,c~ dl"' tie,::' ypc o amp c:
Environmental
__ . Groundwarcr (1)
__ · Surface Water (2)
v .Soil (3)
__ ·,.0th,;_ (4) .·
: .Extractable, . "
Concentrate
__ Solid (5)
__ lJquid (6)
· __ Sludge (7)
--Other (8)
qJT /2
. INORGANIC CHEMISTRY
Time /200
Comments
Total· ' ... ' :
. Pan.meter Reoula mg/1 .. Parameter Results mg/ X,., ·
_._.'Manganese .
✓ .. __ Mercury.
_. _Nitrate
LSc!eni~
< 0. / ·
< 0,? '1
. ORGANIC CHEMISTRY
Parameter. Resula mg/1. :C, . ,.Parameter ·
_·_. :P&T:GC/MS ,. -~-----,· 2::EDB .
__ : Acid:B/N 1:xt· .' _. _, PCB's
__ TOX · . .·. . · _.:_:_Petroleum
MICROBIOLOGY
Par.uneter
_·_Endrin ·
__ .·IJndane
,--. (MF) Coliforrn Colonies/lOOmls .. , ' .,• ..
__ . (MPN) Coliform Colonies/lOOmls _,· ·
Results mg/1
'parameter
__ Gross Alpha
__ ·Gross Beta
• ... ,., ·: --,-----
--: ------·---,-----
. · Parameter . , .. ·. Results mg/1
_· _··-Meth~iychlor ·.·-------
__ · Toxaphen~ i:, ·/
-.-2,4-D
--2,4,5-TP (,U;ex)
RADIOCHEMISTRY
R.;.ults PCi/1
'D"e Received ---------~--------Date Reported __ 9--':_·~yn._._. -~-·-·:-",-_,_· _·°',..•5:?'_:_f ______ _
· Date Extracted---~----~-----'----Dare Anal)-~d -----,----,--'--:--c-:-----~---
Rc=rtcd By -------------'------Lab Number __ L;~''=O~l,...{~)~'1~0.,_._··~1 ·~.:..,. ')t;.. cr'~-tr',-;:· DJ--,--------
,·--.,lt;.bcd
·.•'. :·rlHS JIQJ {Rc-·;,K·J 71.95),
· S..,liJ lnJ H2:.H.:i~us \1/~uc"(Rcvic"".-l/Si) ·
/ !'-: .. C. Department of Human Resources
. O~dsion o( Health Services SAMPLE ANALYSES REQU. Su1e LaOO:.cory o( Public Haith
P. 0. Box 28047
)06 N. Wilrningrnn Street
R.leigh, 276 I I
_s!_:....;dJ=-._/'-U-'-:Z'-o:::.....:3::...:::?__;'2__;:..S-,,_ ____ Field Sample Number -~.l':--r:"-"'c:'--'--Y _________ _
Site Number
Name of Site {..c__.,_A::.u.a ... 1:1=.,f,Je;µ;;oe..lL._~d"'---LJ..O'.r..,.z..1.Lf...cese:...vc__ _____ Site Lo=ion O cl ,-o/ . -d/r Q < .. ~
ID# _--'tf_.,__f ___ Date Colleaed ;z;. >-1 < .Z 0 I 9' J>cf' . · Time ~/_.1...~]~0=---·--'
Environmental.
_·_ Groundwater (I)
__ -Surface Water (2)
V Soil (3) ·
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
--Other (8)
Commenu
INORGANIC CHEMISTRY · .
-Extractablcs -
Par.1meter.
✓ A . ,,.-
--rseruc :'. . .-.'· .. ,
___.L_Barium -\ ': ·
,L Cadmiurit -_. : . /Chr .. -·,'. ;,_.
...JL_ onuum ·
LLcad_-.,,: ,--
./M -.. , , ~ crcury·1,,:·:·
~~Selenium.·,. ·
L-Silver_
--_ Re,ulu mg/1
< o. :J 0 < /. o a -< 0 .Q:L <-o. OD C <o. ;;i o ··
Parameter
✓ Arsenic
..IL.Barium.
,.L.-Caclmium
__ Chloride :; -
LChromium
___ --__ Copper-·
_-_Fluoride --
__ Iron
...L.-Lcad
__ Manganese --
,/ M,;,_cury·
__ Nitrate
./ Sclcni~
-Total
_Resulu mg/~'-_ · ._-Parameter : -,,. . . ' Res ulu mg/ 14;" _
<tQ
J.O . ,, ...
< 0,/
· ORGANIC CHEMISTRY'
Par.a.mete"C Re,ulu.mg/1
_P&T:GC/MS
__ Acid:B/N Exe. ---------'-
_ TOX
MICROBIOLOGY -
Parameter
__ (MF) Coliform Colonics/lOOmls
__ (MPN) Colifon'n Colonics/lOOmls_ -'·'
ParaIDeter
_ EOB
___ PCB's
__ Petroleum
_-_Endrin
__ -Llndanc
D:lte Rcct:ivi;d .-----'----'-----------'--
Rcsulumg/1
Parameter
__ Gross Alpha
__ · Gross Beta
Pan.meter Resulu.mg/1
_: _· _ Metho,cychlor · : :.-...:........:.:....:____c __
_-·-Toxaphcne · . ,_._-'-__:_ __ -__
_·_2,4-D · ·_:. '' ·, .. _, ---'----
__ 2,4,5-TP (sil~~l _-·_--'----
RADIOCHEMISTRY
R~ulu PCi/1 ··
o/-. ,/vie,~·)_ g Dace Reported __ _,_ __ ..:_r_ '.:.....= 1 __ ;::__---'_...:_ ____ _
-Da« Extracted---------------'--------· Date Anal\--d --,-------,------,-----:----------_;__:___
L.b Number __ l_J_,J_l_i:> __ '~l_l_;,,_·,_·",..1.c:;~:_,i:_-; _J..;Jc..·_· ___ _:_;_ __ _ Reported By __________________ _
·~)!"-!$ )101 (Rc\:n,.cd 7185). · .
5,...1\iJ mJ H.i.~rdous Uh He ·c Rcvi~"";-7 /87)
...:. :
•
March 7, 1988
Mr. Jack Butler
TECHlAW INC.
12600 W. COLFAX AVENUE
SUITE C·3IO
I.AKBWOOO, COI.ORADO 8021 S
PHONE: (303) 2,3-1248
•
North Carolina Department of Human Resources
Division of Health.Services
Solid and Hazardous Waste Management Branch
P.O. Box 2091
Raleigh, NC 27602-2091
RE: Channel Master Site, Oxford, North Carolina
Dear Mr. Butler:
I greatly appreciated the opportunity to meet with you on
February 23, 1988 to discuss the Channel Master site. You
provided a helpful background to our site investigation. I also
want to thank you and your staff for copying and promptly sending
copies of documents from your files.
Should any further information come to light with respect to this
site that you feel I should be aware of, I would be very grateful
if you would keep me informed.
Again, your help and cooperation are greatly appreciated.
JL/lkl
cc: Jo-Ann Ward, TechLaw
IF: 144-826
RESTON, VIRGINIA • LAKEWOOD, COLORADO
. .
~. C. Dc;Jar:::1w.1t of Huffian Resources
Division of f1calth Services • SAMPLE ANALYSES REQUES'
Su:e wbomory of PubUc Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 2761 I
si,e Number 3'1 dJ / .z;t :Z. O 3,? 2 S'
Name of Site C/2,al't tld I &at fey
Collected Bat>p/-Ae,,,-, T e..r T,·d)ID# Z' z::
Jo,c,k d/h fie,--
Type of Sample:
Environmental Concentrate
__ Groundwater (1) __ Solid (5)
__ Surface Water (2) __ Liquid (6)
✓ Soil (3) __ Sludge (7)
__ Other (4) __ Other (8)
Field Sample Number ~:J~'f~/ / ____________ _
Site Loca.-ion O -:t7'1, ..-a( , ,d/, C < . ✓
DateCollected @,a, .zs;,;9',£cf' · Time /OJO
a~ .3
eom,~~tCE/V~
I£
' '!.' MAR 3 •;..: ' z
;.--· \ .... -::: . ...
INORGANIC CHEMISTRY
~ SUPERFUND · ~ :-Is,-,. BRANCH ... ~.... .
Extractablcs Total ............ ·,~$•, ; ...
Parameter Results mg/1 Parameter Rcsultsmg/1 · Parameter Resultsffl&/1
__ Arsenic __ Arsenic __ Silver
__ Barium __ Barium __ Sulfates
_·_ Cadmium __ Cadmium __ Zinc
___ Chromium __ Chloride _Ph
__ Lead __ Chromium __ Conductivity
__ Mercury __ Copper _ms -
~ ----~J~_~iuin_ ·-__ Ruoride _TOC
__ Silver __ Iron --
_Lead ----
--__ Manganese --. __ Mercury ----
__ Nitrate ----__ Selenium ----
ORGANIC CHEMISTRY
Parameter
✓ P&T:GC/MS
✓ Acid:B/N Ext.
_TOX
Rcsults.mg/1
. MICROBIOLOGY
Parameter
__ (MF) Coliform Colonics/100mls
__ (MPN) Coliform Colonics/100mls
Parameter
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
Date Received / -d(p -x'. 8'. --;(l.-lv . !,1.)1,-
Dat< Extracted \-d51-~© .
RcportedBv ~/ fa~ w
:,~~s 3101 (R(vi~d i'/SSJ
S..il:J ;inJ H.i:..rdou.s Uhstc (Review 7/87)
Results mg/1 .
Parameter
__ Gross Alpha
__ Gross Beta
Parameter
_·_Methoxychlor
__ Toxaphcnc
_2,4-D
. Results mg/1
--2,4,5-TP (silvcx) _____ _
RADIOCHEMISTRY
Results PCi/1
Purpor.e: Enforcement and compli.l with the N. C. Solid and • Ha:.ardous Waste Management Rules.
P«par.irioJl A .s:imple.analyscs _request form (OHS 3191) must be completed for each type of evaluation requested (e.g., inorganic, organic, microbiology, radiochemistry). For sampling conditions which require more_ than one (I) container (i.e., ground or surface water from landfills) a sample label must be affixed to one of the.containers. The collector must then write the 1itc and sample number on the duplicate. ·
Do not submit an analysis request sheet with no parameters indicated.
Equivalent measureffients:
ppm= µg/ml =mg/I= µgig= mg/kg
ppb = µg/1 = µg/lOOOg = µg/kg
DEFINITIONS/INSTRUCilONS
Site NumbcT -;1.~clve-d.igit site/location identifier, assigned only by the district field representative. ·
Fidd Sample N uinber -A six-digit sample identifier which is pre-printed on the sample label. .. , ., '·• ,,,,. ·, ?ilaip,c'of _Site~ Name of landfill, facility, etc.
• ,;., i' J,•
.-.i~Site l:.ocation. -Address, street number, state road, ere. .•. .. ; ,· ·-
Coll~ed By -Name and ID of sample collector.
Date and Time Collected -Self-explanatory.
Environmental -

A

sample of a naturally occurring substance such as groundwater, surface water or soils which may be contaminated.
Concentrate -

A

sample of a waste, Including but not limited to, sl_udges, resins, treatment effluents or drummed wastes.
. -
Commenta -Lists details regarding sample or sample point, including but limited to, phase separation, ~or ·; odors. ·
Inorganic Chemiatrv-Chcclc ( .,, ) the desired parameters to be ~yzcd. Extractablcs are only performed on a solid or semi-solid. For routine landfill samples, check all parameters in the second and third columns. ·
Organic Chcmiatrv -Chccl:: ( .,, ) the desired parameter to be anal yzcd. If not listed, enter the name in the space provided. . . .
Microbiology and Radiochemistry -The RAieigh office should be consulted prior to sampling for either of these.
Diatribution: I. Original-to State Laboratory of Public Health
Environmental Sciences Branch
· Diaposition:
P. 0. Box 28047·
Raleigh, NC 27611
2. Lab sends copy to Solid and Hazardous Waste Management Branch.
3. Solid and Hazardous Waste Management Branch sends copy to field person.
This form may be destroyed· in accordance with the Environmental Health, Solid and Hazardous Waste Section of the Records Disposition Schduk as published by the North Carolina Division of Archives and History.
Additional forms may be ordered from:
Solid and Hazardous Waste Management Branch
Division of Health Services
P. 0. Box 2091
Raleigh, NC 27602-2091
~-C. Ocpartmc.'.1t of Hu~an Re.sources
Division of Health Services • • State Laborarory of Public Health
P. 0. Box 28047
306 N. Wilm.ingcon Street
Raleigh, 27611
SAMPLE ANALYSES REQUEST
Sire Number sf d) / .z..t 2 O 3,? 2 _s-
Name of Sit• C.6a1-1 tt,2 I da 1 t e y
Collected By Sov1-Rervt T ~ -r,-,,q lD# ¥'f
T fs I 7°'c~ dl11t/-e,? ype o amp e:
Environmental Concentrate
__ Groundwater (1) __ Solid (5)
__ Surface Water (2) __ Liquid (6)
V Soil (3) __ Sludge (7)
__ Other (4) __ Other (8)
Field Sample Number __:::1:...o/.L..!../_,,,'=-------------
Site' --:ion O --r:z':2,.v,,/' , ,4/2 C,: µ.,u,.,. ~
DateCollecred •fe.-t, .zs;,;9'J>JY. Time //00
0-L. IZ-
,.•
Com7k~~, v~
)7, " .\
f, ,I ... ~ ft
O' .. .. i ... '
INORGANIC CHEMISTRY
~ v ~-SUPERFUNO · 4J
--. RDH•~LI .... .. Total Extractablco ~"'14NAGi"'.1/ .,.,. ·~•0-.
Parameter Results mg/1 Parameter Results mg/1 · Parameter Results mg/1
__ Arsenic __ Arsenic __ Silver
__ Barium __ Barium __ Sulfates
_·_Cadmium __ Cadmium __ Zinc
__ Chromium __ Chloride _Ph
__ L,,ad __ Chromium __ Conductivity
__ Mercury __ .Copper _ms -
I _........_~J~.~~U_!Il _ ·-__ Fluoride _TOC
'
__ Silver __ Iron --
_Lead ------__ Mangan~ --
--__ Mercury --
__ Nitrate ----__ Selenium ----
ORGANIC CHEMISTRY ·
1
r ---------------.---'--'-=-_;:,.:.=._;_...:..c:..c.c..c..--.--------'---------i
Parameter
./p&T:GC/MS v Acid:B/N Ext.
_TOX
· Results mg/ 1
. MICROBIOLOGY
Parameter
__ (MF) Coliform Colonies/lOOmls
__ (MPN) Coliform Colonies/lOOmls
Parameter
_EDB
_PCB's
__ Petroleum
__ Endrin
__ .Lindanc
Date Received /-;), &, -'i'? 'f/j,I.J
Date Extracted i-iJ$'il5{::S,I)'\ ~0
Reported By _________________ _
DHS 3101 (Rc,·1!<.-i 7185)
S..1!1.l ~nJ H;,1:;irdous \\-':i.stc (Review /!Bi)
' Rcoults mg/ 1 . Parameter . Results mg/1 • ' -.,,r:t ' i
Parameter
__ Gross Alpha
__ Gross Beta
_· _ Methoxychlor
__ Toxaphene
_2,4-D
-. _ 2,4,5-TP (sil~ex)
RADIOCHEMISTRY
Date Reported ...,,.-,,.-----~~~----------P--,-Bµfl-
Date Analy--.ed ,2-'i!'-li'? 'f1.w" ci!-JtJ-f/(/3~
Lab Number 800.l.29
Purpo..:: Enforcement and compli-with the N. C. Solid • and Ha.:.ardous Waste Management Rules.
P«paratio)l A s.mple.analyses n;quest form (OHS 3191) must be completed for each type of evaluation requested (e.g.; inorganic, organic, microbiology, radiochemistry). For sampling conditions which require more_ than one (I) container (i.e., ground or surface water from landfills) a sample label must be affixed to one of the containers. The collector must then write the aite and a.ample number on the duplicate. ·
Do not submit an analysis request sheet with no parameters indicated.
..--:-:·-~·t--:;-, .... -~ .... ,.-,., .. '! iJ..lt/t··, ....... ·,' '
\
'
-·'-· \
j
Equivalent measurements:
ppm= µg/ml = mg/I =µgig= mg/leg
ppb = µg/1 = µg/lOOOg = µg/lcg
DEFINl'IlONS/INSTRUCilONS
Site Number~ A twclve-<l.igit sitc/loc.ation identifier, assigned only by the district field representative. · r" '..-.'.' · :•.i 1 · Field Sample Number -

A

six-<l.igit sample identifier which is pre-printed on the sample label. ~ .. .. ·-.. ' . .
N;lme of Site .....:·N;me of landfill, facility, etc. . ' . . ), . .\, .'
,, ., -". , . Site(L<x:ati~n'.;··.: Address, street number, state road, etc. . ' .,. . . \ .,·
..... f • .. . ·" e -. :. "1,. . Collccrea .. By -Name and ID of sample collector.
Date and 'lime Collected -Self-explanatory.
Environmental-A sample of a natunlly occurring substance such as groundwater, surface water or soils which may be conta~tcd.
Concentrate-A sample of a waste, including but not limited to, sludges, resins, treatment effluents or drummed wastes.
Comment& -Usts details regarding sample or sample point, including but limited to, phase separation, and/or · odors. ·
Inorganic Chemiatry-Check ( .,, ) the desired parameters to be analyzed. Extractables are only performed on a solid or semi-solid. For routine landfill samples, chcclc all parameters in the second and third columns.'°
Organic Chemistry-Chcclc ( .,, ) the desired parameter to be analyzed. If not listed, enter the name in the spaoc provided.
Microbiology and Radiocheriilitry -The Raleigh office should be consulted prior to sampling for either of these. ·
Dutribuclon: 1. Original-to State L>.boratory of Public Health
Environmental Sciences Branch
P. 0. Box 28047
Raleigh, NC 27611
2. Lab sends copy t'o So)id and Hazardous Waste Management Branch.
3. Solid and Hazardous Waste Management Branch sends copy to field person.
· Dupoeition: This form may be destroyed in accordance with the Environmental Health. Solid and Hazardous Waste Section of the Record, Disposition Schdule as published by the North Carolina Division of Archives and History. ' .....
Additional forms may be ordered from:·
Solid and Hazardous Waste Management Branch
Division of Health Services
P. 0. Box 2091
Raleigh. NC 27602-2091
. ; ~-C. Dc;:iartmc:nt of Human Re.sources • • State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611
Oivisio:, of Health Services SAMPLE ANALYSES REQUEST
Sire Number S1 d) / 2,2 :z_ O 3 tY' .2. _s-
Name of Site C/2aM 11¢ / .da,r fe V:
Collect dB Sov1-Rerv1 Te.s"T,·~ !DI/ '1/-J./-e y
Type of Sample: ✓o,c,.<" dh,tler-
Environmental Concentrate
__ Groundwater (I) __ Solid (S)
__ Surface Water (2) __ Liquid (6)
V Soil (3) __ Sludge (7)
__ Other (4) __ Other (8)
Field Sample Number ..,3«-<o/-'-/-'J=--------------
Site Location O d:Z'1, .,. q( , .A/, 0 < .,
e ' 1me Date Coll cred ,7;,."' .Zs;. I 'l'J>rf' . · T
r.Jff 3
#~£1Vf/J
"
I •• ·-. 0 '"'" z
"' . .. u
0 ;::::
'«>. "':.:.--"~UNO. /;f/ .
INORGANIC CHEMISTRY
~BRANCt1~
fMANAG~
Extractableo
Parameter
__ Arsenic
__ Barium
_·_Cadmium
-. _ Chromium
__ Lead
__ Mercury
•--~foniu_!n __
__ Silver
--
--
------
Parameter
£J'&T:GC/MS
_,,/_ A "cid:B/N Ext.
_TOX
Reoulmmg/1
Reoulmmg/1
. MICROBIOLOGY
Parameter
__ (MF) Coliform Colonics/lOOmls
__ (MPN) Coliform Colonies/!OOmls
-Total
Parameter Reoulmmg/1 Parameter
__ Arsenic __ Silver
__ Barium __ Sulfates
__ Cadmium _·_Zinc
__ Chloride _Ph
__ Chromium __ Conductivity·•.::
__ .Copper _ms .•.
__ Fluoride _TOC
__ Iron --
_Lead --__ Manganese --__ Mercury --. . __ Nitrate --
__ Selenium --
ORGANIC CHEMISTRY
Parameter
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ .Lindane
Resulmmg/1. Parameter
__ Mcthoicychlor
~------__ Toxaphcne
_2,4-D
Parameter
__ Gross• Alpha
__ Gross Beta
--2,4,5-TP (sil~cx)
RADIOCHEMISTRY
-· ~ ;, .........
Rcsulmmg/1
-
-------··
Dare Received __ .1.J_-...,_d"'-'-{"-0_-.1.X:u.[1......-L.J?l"",U./"'0<.... _______ Date Reported =--:----~::-:-::----------p-r t!,A,'P
Dare Extracted \-a'il-~ 1)l'Yl ll0 DateAnalp,d ;1-'if-W-[Ul[" ~-10--Y%8/)
Reported By ________________ Lab Number ____ --,-8_0_0_2_3_0 _______ _
:>!---15-)!01 (Rcv1!<d 7185)
S..1l1J anJ Ha:.Jrdous \\-'a~tc (Review 7/87)
Purpor.<:: Enforcement and compli~ •o,ith the N. • C. Solid and H=irdous Waste Management Rules.
' Prcpar.,tio.n A s:,mple.ana_lvses _request form (OHS 3191) must be completed for each ty~ of ~valuation requested (e.g., inorganic, organic, microbiology, radiochemistry). For sampling conditions which require more than one (I) container (i.e., ground or surface water from landfills) a sample label must be affixed to one of the.containers. The
I
I h··
collecror must then write the 1ite and sample number on the duplicate. ·
Do not submit an analysis request sheet with no parameters indicated.
Equivalent measurc~ents:
ppm= µg/ml = mg/I =µgig= mg/leg
ppb = µg/1 = µg/lOOOg = µg/lcg
DEFINITIONS/INSTRUCTIONS '-· ; r\_ Site Number -A twel~e-digit site/location identifier, assigned only by the district field representative. ·
•,:~ Ficld;~p_l<: ~umJ:,er, -A six-digit sample identifier which is pre-printed on the sample label. ~"-\ J➔-"'·'"l··•. :,~1. . . 'Name of Site -Name of.landfill, facility, etc. ·· .... ··:--~-~),l j ' ' , .
Site Location -Address, street number, state road, etc.
Collected By -Name and ID of sample collector.
Date and Time Collected -Sel£-explanatory.
· Environmental -

A

IWnple of a narurally occurring substance such as groundwater, surface water or soils which may be conta~tcd. ' ·
Concentnte-A sample of a waste, including but not limited to, sl_udges, resins, treatment effluents or drummed wastes.
Comments -Lists details regarding sample or sample point, including but limited to, phase separation, ..;,;y; · , odors. ·
Inorganic Chemiatry-Chcclc ( -' ) the desired parameters to be ~yzed. Exttaetables are only performed on a solid or semi-solid. For routine landfill samples, chcclc all parameters in the second and third columns. ·
Organic Chcmiatry -Chcclc ( .,, ) the desired parameter to be analyzed. If not listed, enter the name in the space provided. . ·
Microbiology and Radiochemiatry -The Raleigh office should be consulted prior to sampling for either of these.
Dutribution: 1. Original-to State Laboratory of Public Health
Environmental Sciences Branch
· Oupooition:
P. 0. Box 28047
Raleigh, NC 27611
2. Lab sends copy to Solid and Hazardous Waste Management Branch_
3. Solid and Hazardous Waste Management Branch sends copy to field =n.
This form may be destroyed in accordance with the Environmental Health, Solid and Hazardous Waste Scaion of the Record., Duposition Schduu, as published by the North Carolina Division of Archives and History.
Additional forms may be ordered from:
Solid and Hazardous Waste Management Branch
Division of Health Services
P. 0. Box 2091
Raleigh. NC 27602-2091
S. C. .Dc;:ianmt;nt of Hu~an Resourc~
Oivisio:; of Health Services • • SAMPLE ANALYSES REQUEST
Sta-:.e Laborarory of Public Health
P. 0. Box 28047
306 N. Wilmington Srrttt
Raleigh, 27611
Site Number _j>'fd)/U2.o3 .f'2.S-Field Sample Number _3~?~/c.....,,-f ___________ _
Name of Sit< .c;.C.,....,,n:.u.'2,cMa...M=d'-'/'--..,A'---"c..,LlOL,,., r ... f,__,e=<.Ly______ Site Lo=ion O 47"2, vef_,, A/r Q ~
So,7',lte,,,_, T ~ -/",·119 ID// 'J'-f Date Collected 1fe .-Z • .Z -S; I 9'",£J"' . Time /,7-00
Jo,c~ dlnfl--e/
Collected By
T fS ype 0 amp e:
/_¢-''YID~ Environmental Concentrate
__ Groundwater (1) __ Solid (5) a_zz /2-
I ,ir ' __ Surface Water (2) __ Liquid (6) .-' .
' ,. ,r,.: ~ ~ V Soil (3) Sludge (7) r -~n 1-.t.t.n i ' \ \ \
__ Other (4) __ Other (8) ~'-M
\~, sui>ERfutlu ,f/ i-
INORGANIC CHEMISTRY . . It-~ a~tlC~..i-~
··• --· -t ... Total -x..!.. l! MAN I>-~ Extractables ,:
Parameter Results mg/1 Parameter Results mg/1 . Parameter Results mg/1 I'
i-
__ Arsenic __ Arsenic __ Silver l .t
__ Barium . __ Barium __ Sulfates . ..
_·_Cadmium _____ Cadmium _Zinc '.
__ Chromium __ Chloride _Ph '
__ Lead __ Chromium __ Conductivity t
__ Mercury __ Copper _ms -!f ~!
• --~kl"!iu.rn ___ __ Fluoride _TOC r:
__ silver __ lron --
--_Lead --
__ Manganese L ----. L.
-·-. __ Mercury ii --!
--__ Nitrate --~!
--__ Selenium --
ORGANIC CHEMISTRY ·.
Results mg/ 1 . Parameter
i
Parameter Resulumg/1 Para.meter . Results ~1,..,
..LP&T:GC/MS _· _ Methoxychlor t
_EDB ' ....,L.. Acid:B/N Ext. __ PCB's __ Toxaphene
_TOX __ Petroleum _2,4-D.
--__ Endrin __ 2,4,5-TP (sil~cx)
--__ Lindane --
. . MICROBIOLOGY RADIOCHEMISTRY
Parameter Parameter ~ultsPCi/1 . , .,
__ (MF) Coliforrn Colonies/lOOmls __ Gross Alpha
__ (MPN) Coliform Colonies/lOOmls __ Gross Bera
----
----
Date Receiv~d I -cJui -'8? Mu Date Reported '
Date Extracted _,~-:a'~~~~~~~lli='-'B~~~------~---Date Analr.ed ra-2? ':t/ll C '3J_t_,_,r~-,.3~
800231 Reported By _________________ Lab Number -----=-=-::.......-------,-----
:1H5 3].::>\ (Rcv1!>e.::l 7185)
S-,_,li-1 ~nJ Ha:..1rdous \'(/:nee (Review 'i/67)
Purpor.e:
P.'C'cpar.,tio..ri
Enforcement and compli.tt with the N. • C. Solid and Hazardous Waste Management Rules.
A .s:,mp.le,analv~ _request fonn (DHS 3191) must be completed for each type of evaluation requested (e.g., inorganic, organic, microbiology, radiochemistry). For sampling conditions which require more. than one (I) conrainer (i.e., ground or surface water from landfills) a sample label must be affixed to one of the containers. The collector must then write the site and sample number on the duplic.are. ·
Do not submit an analysis request sheet with no parameters indicated.
I
. _ ... _.--::. ~~t--: -, . ,/ ·J''' ;.-.:,,.. //' ·,.J .: ' .r /:l;}'
I
Equivalent measurc~ents:
ppm= µg/ml = mg/I =µgig= mg/leg
ppb = µg/1 = µg/lOOOg = µg/lcg
· DEFINITIONS/INSTRUCTIONS
1Slte Number -Ii, twelve-digit site/location identifier, assigned only by the district field representative. · ~. ' .; ', . .
'Fidd Sam.pie NUD1bcr """".. A six-digit sample identifier which is pre-printed on the sample label. '' . \)
Na=;:;f Site,-,. Name of landfill, facility, etc. · •. -..... :.:·11,-:::---,, .. :-..... ·~ . . .
Site Iktio'n"·,r,Addr~; street number, stare road, etc. ·-,..~-, ... 1 ·~ t-'-t,"\ ·:_ ~ . . . . ..
Collected By '...a. Name and ID of sample collector.
Date and Time Collected-: Self-explanatory.
Environmental -A sample of a naturally occurring substance such as groundwarcr, surface water or soils which may be contaminated.
Concentrate -A sample of a waste, including but not limited to, sludges, resins, treatment effluents or drummed -· wastes. . '-.. ··•· .. ~ . .
Coinmenta -Lists Clctails regarding sample or sample point, including but limircd to, phase sq,aratioi>, ~:..-i~:'·; odors. ·
lnorpnic Chemutry-Chcclc ( ✓ ) the desired parameters to be analyzed. Extractablcs arc only performed on a , solid or semi-solid. For routine landfill samples, checlc all paramercrs in the second and third col~· '
Organic Chemutry-Chcclc ( ✓ ) the desired parameter to be analyzed. If nqt listed, enter the name in the ;,p;.;,,.· provided. ···
Microbiology and Radiochemistry -The Raleigh office should be consulted prior to sampling for either . of these.
Distribution: 1. Original-to Stare Laboratory of Public Health
Environmental Sciences Branch
-------1 ... ··• ; .· ,.· . -·-.-·; P. 0. Box 28047 ·
Raleigh, NC 27611
2. Lab sends copy t'o Solid and Hazardous Waste Management Branch.
3. Solid and Hazardous Waste Management Branch sends copy to field person.
· Diapooition: This form may be destroyed in accordance with the Environmental Health. Solid and Hazardous Waste Section of · the :Records Disposition Schedule as published by the North Carolina Division of Archives and History.
Additional forms may be ordered from:
Solid and Hazardous Waste Management Branch
Division of Health Services
P. 0. Box 2091
Raleigh, NC 27602-2091
-~·. C. Dcp"artmc:nt of H11man_ R~ources
.SAMPLE ANALYSES REQU~
State Laboratory of Public Health
Division of He.:lth Services P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611
Site Number st tfJ / u :z. o 3 .? 2 r Field Sample Number l"flr'
Name of Site CnaM #'!1-:# I da,tf@r Site Lo=ion O .x;,4,.,,,/. ,4/, C ,,_
"
Collected By Sovl"herH T .,-r.!Jj. . ID# 4£i Date Collected ,"""h Id, .Zs;,. I 9'J>cf" . Time /2 JO
Type of Sample: 7o,c~ dl~fl-e.,-
Environmental Concentrate I~-/"'. _,~\.\~Ef)n~
__ Groundwater ( 1) __ Solid (5)
__ Surface Water (2) __ Liquid (6) .·, .f!,;-\
V Soil (3) __ Sludge (7) ' -,r.:: "' §
\lt,.i ~ V
__ Other (4) __ Other (8) "' .~~ . t\lt'o o/ ~\l~! .. c~ -~.;;: INORGANIC CHEMIS
Extractables ~ ,.-.NI'-~ p
Parameter Resulu mg/1 Parameter Resulumg/1 · Parameter Resulumg/1
__ Arsenic __ Arsenic __ Silver
__ Barium __ Barium __ Sulfates
_._Cadmium ___ Cadmium __ Zinc ..
__ Chromium __ Chloride _Ph
__ Lead __ Chromium __ Conductivity
__ Mercury __ Copper . _TDS
--~foniu_!n ___ __ Fluoride _TOC
__ Silver __ Iron --
--_Lead --
----Manganese ---
-·-__ Mercury --
--__ Nitrate --
--__ Selenium --
ORGANIC CHEMISTRY
Parameter Resulumg/1 Parameter Results mg/1 Parameter Resulumg/1
~P&T:GC/MS _EDB --Methoxychlor
__ Ac1d:B/N Ext. __ PCB's __ Toxaphene
_TOX __ Perroleum _2,4-D
--__ Endrin __ 2,4,5-TP (sil~cx)
--__ Lindane --
MICROBIOLOGY RADIOCHEMISTRY
Parameter Parameter Resulu PCi/1
__ (MF) Coliform Colonics/lOOmls __ Gross Alpha
__ (MPN) Coliform Colonies/lOOmls __ Gross Beta
----
----
Date ReceivC:d L-J.(, -'lR" :tJ.0.1 Date Reported
Date Extracted \-~7>1Yl EJuJ PT t})./f} .
Date Analr.ed .i.-'i?-'Ffl.':lM.ir ,l;.-tl-f« 13/)
Reported By Lab Number 800232
DHS )!QI (Rev1s.cd 7185)
Soli.l ;r,nJ Ha;:.a.rdou.5 Waste (Review 7/87)
Purpooc:
Pcep"r;irioJl
Enforcement and compli•-with the N. C. Solid and Hazardous -e Management RWes.
A s:,mp.le.anaJv~_requcst.form (OHS 3191) must be completed for each type of evaluation reque,ited (e.g.,
inorganic, organic, microbiology, radiochemistry). For sampling conditions whkh require mo~tthan one (1)
container (i.e., ground or surface water from landfills) a sample label must be affixed to one of'th'd'2B~tainers. The
collecror must then write the aitc and sample number on the duplicate. ·
Do not submit an analysis request sheet with no parameters indicated.
/
'
Equivalent measurements:
ppm= µg/ml =mg/I= µgig= mg/leg
·;·--,_ ppb = µg/1 = µg/lOOOg = µg/lcg
DEFINITIONS/INSTRUCTIONS
Site Nuinbtt -A twe!ve--digit site/location identifier, assigned only by the district fidd representative. 1 · _, ,. ... • • .
Field Sample ~ umber -A six-di~t sample identifier which is pre•printed on the sample label.
•. .... .-: • ;_ t·
Name of Site-;-Nam'e•oflandfill,-facility, etc.
Site Location·:;· ~~d&~~:~1
~eet ~u~ber, state road, etc. , .;.,'_ ,,,.l., r; , ,
Collected By -Nime and ID of sample collector.
Date and Time Collected -Self--cxplanatory.
Environmental -A sample of a naturally occurring substance such as groundwater, surface water or soils which
may be contaminated.
Concentrate -A sample of a waste, including but not limited to, sludges, resins, treatment effluents or drummed
wastes .....
Commenta -Lists details regarding sample or sample point, including but limited to, phase separation, and/or ;
odors.
Inorganic Chemiltry -Checlc ( .t ) the desired parameters to be analyzed. Exrraaables arc only performed on a
solid or semi-solid. For routine landfill samples, checlc all parameters in the second and third columns. ·
Organic Chemiltry -Checlc ( .t ) the desired parameter to be analyied. Hnot listed, enter the name in the space
provided.
Microbiology and Radiochemistry -The Raleigh office should be consulted prior to sampling for either
of these.
Dutriburion: I. Original to State Laboratory of Public Health
Environmental Sciences Branch
· Diaposirion:
. P. 0. Box 28047
Raleigh, NC 2 7611
2. Lab sends copy to Solid and Hazardous Waste Management Branch.
3. Solid and Hazardous Waste Management Branch sends copy to field person.
This form may be destroyed.in accordance with the Environmental Health, Solid and Hazardous Waste Section of
the Record, Disposition Schedule as published by the North Carolina Division of Archives and History.
Additional forms may be ordered from:
Solid and Hazardous Waste Management Branch
Division of Health Services
P. 0. Box 2091
Raleigh, NC 27602-2091
DIVISION OF liI.AL rrl SERVICES
SO~AJ,'D HAZARDOUS 1-lASTE MANAGE!£K-RANCH
Chain of Custodv Record
Hazardous 1-laste Materials
Location of Sampling: / Generator
__ Storage Facility
Other:
· __ Transporter __ Treatment Facilit}
__ Disposal Facility __ Landfill
-----------------------
Company's Name LiaJ1>1el ct«sfey
Address O ,k-,,,c'o r ol I N, c..,
✓ .
Collector's Name SZerz:ti./4-~✓
c7 signature
'
Date Sampled J;,,1-1 ZS' /9'??
Telephone( Cf/'!) Cf J ~ -"/ 7 //
Tele_phone('f'/o/ )7) J-Z.tf'O /
-·
Time Sa.mp
Type of Process Genera ting 1-laste,..L../'X_.:_.E-e:::..:..Ti..::ci~/'....--!e~:..L1/,.::!q:.L..L.!:.l..~H,"t-------,--+--
' . Field Information
·Field Sample No. J'fl/
Chain of Possession:
1-.~~/ c>. signature
2.
3.
signature title inclusive dates
Results reported
sigr,ature title_ date
Instructions: Complete all applicable information including signatures, and
submit ~ith -.analysis request forms.
BASE/NEUTRAL AND ACID
EXTRACTABLES
aJl1POUND
• • STATE LABORATORY Of PUBLIC HEALTH
DIVISION Of HEALTH SERVICES, N.C. DEPARTl1ENT Of HUMAN RESOURCES
P.O. BOX 28047 -306 N. WILHINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEHICAL ANALYSIS
LAB NO tr 1J oJ.;;i.x Jl'l)O;).;).."i voo.:J..~D f?O 1:,;l?, l
FIELD# ;=;q ti 3a, /,), ~ cyj? 3 "/ I if-
TYPE ( _, (3 f 3 l f 3 l
'S?O O::l.-=12.
.~9/S-
( 31 )
UNITS ,,a/ ll ua/ka ,;n;tl( .. nika) .=...lr,";'n/ka 'm-1.:l(µq/kg) .. nl!J/2,;/kd un/ l un/kn
N nitrosodimethvlamine I I\/ .('fi, u..,. LA..... ' , ' , U--
bis (2-ch loroethvl )ether
2-chloroohenol
ohenol
l 3-<lichlorobenzene
l 4-<lichlorobenzene
l 2-<lichlorobenzene
bisf2-chloroi l )ether
hexachloroethane
N-nitroso-di n...nrnnvlamine
nitrobenzene
i"-lY'lhorone
2-nitroohenol
2.4-<limethvlohenol
bis(2-chloroethoxv)methane
2.4-<lichlo~henol
l 2 4-trichlorobenzene
nanhthalene
hexachlorobutadiene
4-ch l oro-m-creso l
hexachlorocvclooentadiene
2.4.6-trichloroohenol
2-chloronaohthalene
acenaohthvlene
dimethvl ohthalate
2.6-<linitrotoluene
acen.::1nhthene
2,4-<linitroohenol
2.4-<linitrotoluene
4-n i trooheno l
fluorene
4-chloroohenvlohenvlether
diethvl ohthalate
4,6-dinitro--o-cresol
diohenvlamine
azot>enzene
4-br""""'henvlohenvlether
hexachlorobenzene
=ntachlor=henol
ohenanthrene
anthracene
dibutvl ohthalate
fluoranthene
J -Estimated value.
SO/J't,.SO
l()l.'~:io
-ro/t~.~o
IO/:Z30
. ,
So )~,,,,
I
J,,
I 11 /.330
/," /;/~I'
so/11,,:ro
I/I l~.'~D
~,
rn1) L
f(,_O/SOIL-
I
I
.J.t
K -Actual value is known to be less than value given.
I
" I
L -Actual value is known to be greater than value given.
U -Haterial was analyzed for but not detected. The nurber
NA -Not analyzed.
1/ -Tentative identification. £1 -On NRDC List of Priority Pollutants.
N.C. V~v,u.,~on 06 Hea,Uh Sv,_vi~r,,1
VIIS 3068-0 I 4 I 86 Labol!.a.,to1u;)
--./ .. , . 'vr---:,, -."-ll ' I .r \
\
' i'i I _M~ " t:' V s....:-,
I"' .... , \'NI ~-'. . -"'fli1'i'i.,; --~
, ~ ,,.,~, -
-' , ..... ,,
is the Ninirrun Detection Limit. ()1 l) L-
BASE/NEUTRAL ANO AC 10
EXTRACT ABLES
aJNPOONO
ovrene
benzidine
butvl benzvl ohthalate
benz(alanthracene
chrvseoe
3 3-<lichlorobenzidine
bi s(Z-,,thvl hexvl l nhtha 1 ate
di-n--0etvl nhthalate
benzo(blfluoranthene
benzo(kl fluoranthene
benzo(alnvrene
i ndeno( l. 2 3-<:dlnurene
dibenzo(a.h)anthracene
benzo(a.h il=rvlene
ani 1 ine
benzok acid
benzvl alcohol
4-<:hloroaniline
dibenzofuran
2-<rethvln•""thalene
2-<rethvlohenol
4-<rethvlnhenol
2-ni troani line
3--ni troani line
4-nitroani line
2. 4 5-tri ch lo~heoo 1
J -Estimated value.
• • STATE LABORATOOY Of PUBLIC HEALTH
OIV!SlON Of HEALTH SERVICES, N.C. DEPARTMENT Of IIUKAN RESCXJRCES
P.O. BOX 28041 -306 N. IIILMINGTON, SI., RALElGH, N.C. 21611
OOGANIC CHEMlCAL ANALYSIS
LAB NO 5i' oocRol1t fi'9([1 "\9 Y no-A -=io X ,:Jo;)? I
FIELD # -:zq I J -:,,q, .1 . ~QI _i -~ q J I/
TYPE ( -:: l ( '21 ( .::r) ( -, , l
UNITS uofal(' ,intkO\ uol'lt'.t•n/ka nn/ctL~/kol .. nfM " 10/:,::v, , . . , .,, '(' i'IC I
..-,, i,1.<o // ... ,. -
10/.:"'0 .· I tr
I i
. ' ' ::.:.· .. -
,SOI ,,_ ,:,, ,i,\ "'""
, -, "'3" ,;. \
107.Iio \"', -----·
so~·· .,..,.,
.... ~-
• i,, ,, " ' , ,/
<o 7,,,.:-r 1/4-I.,(._,. I.A..-, IA_,.
,T,
I" h:io
. -
S'ol,,A<o
,J '-" -..I' ' ,
lo be less than value given.
~ooa.=
.~"i)..l
r ~ l
· · r /kal
I-I 11L ~
--.... '\. . \
\
I -" 171
,'
~ ... -:
., ~'l
. /
VL..
.,,
K -Actual value is known
L -Actual value is known
U -N.aterial was analyzed
NA -Mot analyzed.
to be greater than value given.
for but not detected. The nuioer is the Minirrun Detection Limit. /YI i)L
1/ -Tentative identification. gt -On NROC List of Priority Polluldnls.
t-J. C. D,{,v,l/2.(.0,1 u 6 Hc.ciUh SeJlv.t<:c.,)
DHS 3068-0 (4/&6 I.abo'1.alo!J.if)
( )
uo/} un/ka
' '
l'tRIGEABLE CCl'froJNOS
00'1f'IJIJHO
chloranethane
brarcmethane
dichlorodifluoronethane
vinvl chloride
chloroethane
rrethvlene chloride
trichlorofluoronethane
ethene I 1-dichloro
ethane. I. 1-dichloro-
1-2-trans-dichloroethene
chloroform
ethane 1 2-dichloro-
ethane I 1. 1-trichloro-
carbontetrachloride
brorodichloronethane
nrnru.ne_ 1.2-dichloro-
1.3-trans-dichlo,
trichloroethvlene
chlorodibrooonethane
benzene
ethane 1-1 2-trichloro-
l .:H:is-dichlo1 ne
2-ehloroethvl vinvl ether
brorofonn
ethane. 1. 1 2 2 tetrachloro-
ethene tetrachloro-
toluene
ch lorobenzene
ethvlbenzene
acetone
2-ootanone
carbondi SUI fide
2-hexanone
4-<rethvl-2~ntanone
stvrene
vinvl acetate
xvlenes Afal'I
J -Est1m>ted value.
• •
STAIE LABORATOOY Of PUBLIC HEALTH
DIVISION Of HEALTH SERVICES, N.C. 0£PAAIM!:NT Of HUIWI RESOJRCES
P.O. BOX 28047 -306 N. WILMINGTON, SI., RALEIGH, N.C. 27611
OOGAHIC QjEMlCAL ANALYSIS
LAB NO Oh~ -,-,9. l? n/) 1 :)9 f'i lllr\----::::;.-230 9/V',;22,1
FIELD I
TYPE C 3 l ( .3 ) I 3 I C 3 l
UNITS . ""/kn _,c,1 ,uo/ko .. ...LV:-,n/ko ,.....,_, .r.;;/ko
JO LA_ , ' ,-
IV ,I, \ '
'2-.£) /+) * ,..1. ·,-1'-(J: ~
,o (_,<.., I.A__ U,
10 I
'i? I'\/> ., '2 ...,
I .,3 l
-.<,;/ko
I '
!, /.,, ,er '-II/~
;i.o ~~ \'" 'C..l,
~ I
l ' I I .,
! :n ' ' ''"' ., . , _-.,
w ,.. '
C)
-~ -~ -,.., ,._ ,n .,.! -. '·~
'
J
..::-
·, ' I I '
)() ,._ (A_..., u....-363 LL-
/0 I '
5
/CJ
/0
5
/0 '
', ',/ ' , I
l'Vi'"
, •• In
' V
to be less than value given.
( l
• ··"/I un/ko
' '\
1
..
~
t.,'
","J
,;,,,
K -Actual value is known
L -Actual value· is known
U -l\aterial was analyzed
NA -Not an.,lyzed.
to be greater than value given.
for but not detec led. The ntnber is the HinitT'l.Jll Detection Limit. = l'??iJL
1/ -Tentative identification
~I -On NROC List of Priority0 Pollutants.
N.C. Division of llealtt1 Services
IJIIS 3068--0 (4/86 Laboratory)
+. ' cl, ch. lorocl, { Luo rom e:1-/-\.a..l'UL -
I a. b co h +a iY\. i 11.a.,+;0 n
• •
26 February 1988
TO: File
FROM: Jack Butler
RE: Telephone conversation with Falecia Barnette, U.S. EPA (404-347-2234)
about Channel Master, NCD 122263825.
Ms. Barnette was contacted on this date to determine if she had
received a copy of Dixie L. Laswell, Gessler, Glynn, Laswell, Fleischmann,
Hughes, and Socol, Ltd. letter of February 17, 1988. Ms. Barnette reported
that she had not seen a copy of the letter, however, since Giezzelle Bennett
had seen the letter it should be in the file and we do not need to send a copy.
JB/pb/0543b.36
• •
26 February 1988
TO: File
FROM: Jack Butler
RE: Telephone conversation with Roger Coasts, Channel Master (919-934-9711), about the Channel Master site, NCD122263825.
Mr. Coats contacted the N.C. CERCLA office on this date to give an update on the subject site. Because of the recent wet weather the lagoon area is still too wet to continue digging in. Mr. Coats and I agreed that it was more important to get the contamination level down to the levels attained in quadrants III and IV than to rush into filling the lagoon.
JB/pb/O543.37
• •
25 February 1988
TO: File
FROM: Jack Butler
RE: Telephone conversation with Giezzelle Bennett, U.S. EPA (404-347-3402) about Channel Master, NCD 122263825.
Ms. Bennett was contacted on this date to determine if she had received a copy of Dixie L. Laswell, Gessler, Glynn, Laswell, Fleischmann, Hughes, and Socol, Ltd. letter of February 17, 1988. Ms. Bennett reported that she had a copy of the letter, however, it was not EPA's policy to hold meetings as requested in this letter or respond to letters such as this at this stage of a project.
JB/pb/0543b.33
• •
24 February 1988
To: File
From: Jack Butler
Re: Channel Master, NCD122263825
On February 17, 1988 I met with Al Hankey, Dick Green, and Pat Cwieg,
EPA Region IV, to discuss the status of the Channel Master site in Oxford, N.C.
JB/pb/0543b.26
-:(_ C. 0:-:;J:..":'::r.:..-nt of Hum.an Resources
Oivisi,):i of+:caltli"Scrviccs .AMPLE ANALYSES REQUES.
Sta:e Laborarory of Pu:Jlic Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 2761 I
Sire Number ,,,3',___°l_dJ_I_Z_-:7-_~--=b~)'--.?."--'-~----"'"-----Field Sample Number __,_J~o=-~tr~2...=---------
Name of Site _,-,c..,,C,<.L/2,__,,,ac,,,,.c..c..J!C-'e .. -c,1_ ... d<'---''--'O(~~.£,.._Z,,_.e=r-____ Site Loca.-ion t7x/l;~ &,-C _,
:Ollected By V, £, £Jc( f/e.r: lD/1 '3/ ~ Date Collected /1/41 .,, :J.-.0, l'o/,P-7 ·
. . ;, Time /0/00
Type of Sample:
Environmental
__ Groundwater (I)
__ Surface Water (2)
~ Soil (3)
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
L
INORGANIC CHEMISTRY
Extractables
Parameter
__ Arsenic
__ Barium
_·_Cadmium
__ Chromium
__ Lead
__ Mercury
:__,...;__~k-~~U,!_l\_ --
. _._-Silver
Results mg/1 Parameter
__ . Arsenic
__ Bariwn
__ Cadmium
__ Chloride
__ Chromium
__ .Copper
__ fluoride
__ Iron
_Lead
__ Manganese
__ Mercury
__ Nitrate
__ Selenium
Resultsmg/1 Parameter
__ Silver
__ Sulfates
__ Zinc.
-Ph
--Conductivity _·_ms
_TOC
Rcsultsmg/1
ORGANIC CHEMISTRY
Parameter
7,& T:GC/MS
__ Ac1d:B/N Ext ..
_TOX
Parameter
Rcsultsmg/1
MICROBIOLOGY
__ · (MF) Coliform Colonies/lOOmls
__ (MPN) Coliform Colonics/lOOmls
Parameter
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
Rcsultsmg/1
Parameter.
__ Gross Alpha
__ Gross Bera
Parameter
--Methoxychlor
--Toxaphcnc
_2,4-D
--2,4,5--TP (silvex)
RADIOCHEMISTRY
Resultsmg/1
Results PCi/1
Date Received -~' _I -~d-~0~-'6~'7'-',&...,_'A=~----~---Date Reported -:,----;-;;---;~;=..--"~-:=J7"'c=.~-'J/'---------
/3t-'f+. fT
Date Analyu:d --'--l---'/.}."---"-'l!-"-S,_,8_,..Q'---...=~/7-~/;c;'f;-""'.·-:!'-'l-"-?:_:t1:zw./1..J [!...._ __ _
703224
Lab Number ---------------,-----
I· 1).-['8' 15 ,:_9
Date Extracted--..,,.----,,,,.----------~---
Reported By £J IL C NJ--
[)HS 3\01 (Rcv1s.cd 7185)
5,..ili.l .inJ H:.1:.:irdous \'(/;isrc (Review 7187)
Purpose: E_nforccment and complian.th the N. C. Soli_d and H=rdous W.Management Rules.
..'!'
Prcp;\r,ltio.n A s'lmpJe.ana_lysc,s _request form (DHS 3191) must be completed for each ryp,, of ~valuation requested (e.g.,
inorganic, organic, microbiology, radiochemistry). For sampling conditions which require more than one(\)
container (i.e., ground or surface water from landfills) a sample label must be affixed to one of the containers. The
collecror must then write th_e aite and aample number on the duplicate. ·
Do not submit an analysis rcqucsr sheet with no parameters indicated.
·"' .,•;~ .. \•#-T;·•·:,,,... Equivalent measurements: .•. ,·,, .•• .1,-;--.... "' ,, \ ., .. J,,.., µ '
·· · '1 \ ppm= µg/ml = mg/1 =µgig= mg/leg
··v \ ·, ppb = µg/1 = µg/lOOOg = µg/lcg
. \
: , :· ··.·: :-:-· _,':,' ·: ':') DEFINITIONS/INSTRUCTIONS . -
Site N~mber -'A twclve-<ligi~ ~t'\iflocation identifier, assigned only by the district field representative.
•.· . nl .
'Field'Samj:,lc Number,+,;A six,digit sample identifier which is pre-printed on the sample label.
•·· .. ,, ···.;, ··,'.!•'!": •• -~'"/ . .
Name of Site _.: Naine of.laiidfill, facility, etc.
Site Locati;~· ~ia:~:':cet number, state road, etc.
Collected By -Name and ID of sample collecror.
Date and Time Collected-Self-explanatory.
Environmental-A sample of a naturally occurring substance such as groundwater, surface water or soils which
may be contami;,,,tcd.
Concentrate -A sample of a waste, including but n~t limited to, ·sludges, resins, treatment effluents or drummed
wastes.
Comment& -Lists details regarding sample or sample point, including but limited to, phase separation, and/or
odors. · ·
Inorganic Chemutry-Checlc ( ✓ ) the desired parameters to be analyzed. Exttactabies are only performed on a
solid or semi-solid. For routine landfill samples, chcclc all parameters in the second and third columns.
Organic Chemutry -Checlc ( ✓ ) th~ desired parameter to be analyzed. If not listed, enter the name in the spaoc
provided. · ·
Microbiology and Radiochemiatry -' The Raleigh office should be consulted prior to sampling for either
of these.
Dutribution: 1. Original to State Laboratory of Public Health
Environmental Scicnocs Branch
' · Dupooition:
P. 0. Box 28047 ·
Raleigh, NC 27611
2. Lab sends copy to Solid and Hazardous Waste Management Branch.
3. Solid and Hazardous Waste Management Branch sends copy to field person. .
This form may be destroyed in accordance with the Environmental Health. Solid and Hazardous Waste Section of
the Records Disposition Scheduk as published by the North Carolina Division of Archives and History.
Additional forms may be ordered from:
Solid and Hazardous Waste Management Branch
Division of Health Services
P. 0. Box 2091
Raleigh, NC 27602-2091
t..~ C. Dcp~~:rnc.-nt of Human Resources .AMPLE ANALYSES REQUES. State Laboratory of Public Health
Divisbn o( Health Services P. 0. Box 28047
306 N. \l:7ilmington Srrect
Raleigh, 276 I I
S;te Number J o/ dJ / z -;Z.:Z b.) J>hS" Field Sample Number 3 £)(; :J
Name of Site 411 CA o,,n t!.e-/ Aots7e.v Site Loccion L7 x7'1,YpS A/,C,,
V, ~-£f.,, r/ec. ~~ .A/ • .,_ '2..0 lo/f"7 · '0/30 .
::Ollecred By ID# Date Colleaed
. / itCEfv£~ r ype of Sample:
Environmental Concentrate Commen
~ s,,fe A'// __ Groundwater (1) __ Solid (5)
__ Surface Water (2) --Liquid (6) ~ .:,./ :J. .i /f'l, ... ,,. 0
~ Soil (3) __ Sludge (7) ,~ ~)
. ~-SUPERFUNO '.fl
__ Other (4) __ Other (8) ..,. ____ :__ ·"
~ANA~t~3/
INORGANIC CHEMISTRY
Extractablcs Total
Parameter Results mg/ 1 Parameter RC&U!ts mg/1 Parameter Results mg/1
__ Arsenic __ . Arsenic __ Silver
__ Barium __ Barium __ Sulfates
_._·_ Cadmium __ Cadmium __ Zinc.
__ Chromium __ Chloride __ Ph
__ Lead __ Chromium __ Conductivity
__ Mercury __ Copper _·_ms
~-s~J~.11i_u_rn_ ·-__ Fluoride _TOC
_. _Silver __ Iron .. --
__ Lead ----
----Manganese --
--__ Mercury --
__ Nitrate ----__ Selenium ----
ORGANIC CHEMISTRY
Parameter Results mg/1 Parameter Results mg/ 1 Parameter Results mg/1
~&T:GC/MS _EPB __ Methoxychlor
__ Acid:B/N Ext .. __ PCB's __ Toxaphene
_TOX __ Petroleum _2,4-D
__ Endrin --2,4,5-TP (silvex) --
·--__ Lindane --
i
MICROBIOLOGY RADIOCHEMISTRY
.
Parameter Para.meter. Results PCi/ 1
__ · (MF) Coliform Colonies/lOOmls __ Gross Alpha
__ (MPN) Coliform Colonies/lOOmls __ Gross Beta
. --------
Date Receiv~d /l-.;1.o-w1 iX5 Date Reported t3/Jt/-. pr
Datt" Extracted /-IJ--i'Y f5!) Date Analy:ed L-IJ.-Wl?!J 1-1+i'% -yu.v ?O.J~~is
Reported By Lab Number
OHS J\OJ (Rev1scJ 7185)
$..lb,! .anJ H.i::.'.!rdous \\-':ntc (Rc\·ic.,..· 7/87) I I
Purpose:
·P--rcpaTTltiOJl
·. E.nforcement and compli .. ith the N. C. Soli.d and Hazardous \':<. Management Rules.
A sam:,Je.ana_ly"°"·request form (OHS 3191) must be completed for each type of evaluation requested (e.g.,
inorganic, organic, microbiology, radiochemistry). For sampling conditions which require more than one (·1)
container (i.e., ground or surface water from landfills) a sample label must be affixed to one of the containers. The
collecror must then wrire th.e aite and sample number on the duplicate. ·
. ,·Do·not,submit an analysis request sheet with no parameters indicated. ,,..~·~\j \ :i:J.1;1"-. . . . Eq. • ·1
;1 ·'-,) .~ -1 '\ wva ent measurements:
J \ I ... ppm= µg/ml = mg/1 =µgig= mg/kg
ppb = µg/1 = µg/lOOOg = µg/kg
' ·-,,.:-: . , t',.d , , • I . -, ,. '.~ ~ 1_;;
• • ~, DEFINITIONS/INSTRUCTIONS \ . .. '
..;~,. .Site l':/umbeT ?1 A twelve-digit site/location identifier, assigned ocly by the district field representative. \ .'>. (!b· .. ~~-. : ~.; . .~:/ -
',\;_. lFidd·Sain. q _p,e Number -A six-digit sample identifier which is pre-printed on the sample label._ "'.J.-.. .... .1'-\•t.,' . . •• ~Nme of Site -Name of landfill, facility, etc.
Site Location -Address, street number, state road. etc.
Collected By -Name and ID of sample collector.
Date and Time Collected -Self-explanatory.
Environmental - A sample of a naturally occurring substance such as groundwater, surface water or soils which
may be contami;,,.ted.
Concentrate-A sample of a waste, including but n~t limited to, ·sludges, resins, treatment effluents or drummed
wastes.
Commcnt1 -Lists details regarding sample or sample p,~int, including but limited ro; phase separation, and/or
odors. · ·
Inorganic Cheomtry -Chccl:: ( ~ ) the desired parameters to be analyzed. Extractabics are only performed on a
·solid or semi-solid. For routine landfill-samples, chcclc all parameters in the second and third columns.
Organic Cheomtry -Chccl:: ( ✓ ) the desired parameter to be analyzed. If not listed, enter the name in the space
provided. · ·
Microbiology and Radiocheomtry -' The Raleigh office should be consulted prior to sampling for either
of these.
Dutribution: 1. Original to State Laboratory of Public Health
Environmental Sciences Branch
· Duposition:
P. 0. Box 28047
Raleigh, NC 27611
2. Lab sends copy fo Solid and Hazardous Waste Management Branch.
3. Solid and Hazardous Waste Management Branch sends copy to field person. .
This form may be destroyed in accordance wid.1 the Environmental Health. Solid and Hazardous Waste Section of
the Re:ords Disporirwn Schd..le as published by the North Carolina Division of Archives and History.
Additional forms may be ordered from:
Solid and Hazardous Waste Management Branch
Division of Health Services
P. 0. Box 2091
Raleigh, NC 27602-2091
. I
• i
DIVISION OF
SOLIW HAZARDOUS
EEJ..L To. SERVICES
WASTE MANAGEMENT
E
Chain of Custodv Record
.,. ~dts/i'<
Hazardous Waste Materials 0 l Z ~ 8
Location of Sampling: i. SOPl:f!FUNi) ,f'
Generator __ Transporte ~~~:RAN~ attnent Facility
Storage Facility Disposal Faci AGi andfill
.,/Other: C,4:;&c1,AC/ea,0·-4"AO ---v
Company's Name CAor11ne,I Aa s::f-er
Address s,,.,,,,,~t-A✓-·e,/4,I I ,4/,C /
Collector's Name .;;:;~
U · signature
Date Sampled A/ov, 7-0. l7S:1 J
Telephone(9'1z' )"fJ<;&-r7/J
Tele_phone( o//o/ ) 7 J .r-2. fO /
TiIDe Sampled /0 -// d, fl,
Type of Process Generating Waste . ...::;.4....__.,.e-"-"'-V...:q:,.,/.____.._(8__,_¼;:;.a....._f...:,_·;...,1-r-~_._, _________ _ -/
. Field Information
. ·Field Sample No • .) f?'C 2
Chain of Possession:
l.Gg~~ · signature titl:e /U>v-2~/Cff'.7
inclusiv'e dates
2.
signature
fhom .lbw~<((-fa Jl-;;_o -~"?
title inclusive dates
3.
signature title inclusive dates
Results reported
sigr1ature title date
Instructions: Complete all applicable infcrmation including signatures, and
submit ~ith·~nalysis request forms.
✓.:.':,;,\ \ -i.) :Jc}·-.. DI\'IS. ION· o-E-: •· -r-.: s-:R\1IC"'S ~ (\ .. , '1 •··· ... 1¥•1 " t ~.L ... -~ ...
_/ \.,... SOLID ·-~HAZARDOUS \./ASTE l'.ANAGEMENT B. . ·I
i , , , eceipt. for Sanmles . I ·.1, / i, •• \ '"
The samples i describec:·· b~i~~ wer'e · collected in connection with t:he adminis·tration;
enforcemend'tand documentation :it the: \"~~i\ ··,1.•: .;ict-·~··tt~r;:! _}~~/
( ) North Carcilina''Eaziddous,.Waste Management Rules, 10 NCAC 10:F ... ,.,. __ ::•;~ .• ;-! •• ,i,,, ..... : .,;_-... ·-::/
( ) North. Caroli~:::IS&l'.fd:.t·~~~e Management Rules, 10 NCAC l0G
() Comprehensive Environmental Response, Compensation and Liability Act: (CERC"'i.A)
( ) Toxic Suostarices Control Act (TSCA).15 U.S.C. §2601, et·~-, specifically
Section ll_of TSCA,. 15 U.S.C, @ 2610.
Inspector.' s Name Inspector's Address
Name of Firm Fi= Address
Firm .Owner, Oprc.:·a ~er, or Agent Title
----.--------,-------------,-------------,----------·
SAMPLEi--~c~o~L~L7E~C~TED~-=-~I -;-;-;--;;~SAMP:;=-=~L~E;;--=TYP,=-;:~E=-;::-t--;=~·~D~u~?7·,7Ic~A~T~E:;;;:;:s~AMPLE:r.::~~s=;:;:;-lt-;:~s.i~A-~~~~;E~L=o~c,=,~·r~1~o~N=-_
NUMBER DATE TL>£ I \./ATER SOIL ortl~R O:rERED1AcCEPTED REJECTED! o~:srnl O::-SITE
I i I
Receipt for the sample(s) described.
above is hereby ackno·-·ledged:
Signature of Inspector
Title
I I
I I I
I
Receipt/rejection of duplicate or split
sa:::;les is hereby ackno,dedged·:
Signature of Firm Cr.mer, Operator, or Agent
C0M!1ENTS. __________________________________________ _
•
BASE/NEUTRAL ANO ACID
EXTRACT ABLES
COl1POUNO
N-nitrosodirrethvlamine
bis(2-ch loroethvl )ether
2 ch 1 orooheno 1
ohenol
1 3-<lichlorobenzene
1 4-<lichlorobenzene
1.2-<lichlorobenzene
• • STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
LAB NO r1 cJ 3 Z.. LL/· '7 I) ;i .:i. z;;
FIELD# 3 '>lh-z. .37;~3
TYPE ( :'3) ( 3) ( ) ( }
UNITS .--.n r.:_11 .. n/kit-' w:,7.1 ('uail<Q" ua/1 ua/ka un/1 un/ko
/()/ ,,,.,, U-~
I
/
I , I
bis/2-chloroi llether ~
hexachloroethane
N-nl troso-di -n ....nrrv,,vl amine
ni trobenzene
icnnhorone
2-nitroohenol
2.4-<lirrethvlohenol
bis(2-chloroethoxvlrrethane
2.4-<lichlo~henol
1.2.4-trichlorobenzene
n•nhthalene
hexachlorobutadiene
4-chloro-m-<:resol
hexachlorocvclnn<>ntadiene
2.4.6-trichlo~henol
2-chloronanhthalene
acenanhthvlene
dirrethyl ohthalate
·2.6-<linitrotoluene
acen.:.nhthene
2.4-<linitroohenol
2.4-<linitrotoluene
4-nitroohenol
fluorene
4-chloroohenvlohenvlether
diethvl ohthalate
4.6-dinitro-o-cresol
diohenvlamine
dZobenzene
4-brnmnnhenvlohenvlether
hexachlorobenzene
=ntachlor~henol
ohenanthrene
anthracene
dibutvl ohthalate
fl uoranthene
J -Estimated value.
SOI, "-"O
IIO/.'l"IO
.,;0/11~-:o
/0/330
,,
.. 01 //,.('/";
~,
//l, -~30
,,,1.$3n
S"0//0S"O
J/1 ,-:ru,
\
rn1>L
f{.,_o/SOIL-
-.J.I
K -Actual value is known to be less than value given.
r-
~~
,,
I l ( l
un/ 1 un/ko un/ 1 un/ko
"'o{.. l'.t-I Vl' ;:,,,._
" ~, ,/ " . \. ,
.. -• '-'-<I xq . • z
~ _,.,,
~---: ·=~---·.· .... "'7 --~
l -Actual value is known to be greater than value given.
U -Material was analyzed for but not detected. The nUTt>er 1s the_HinilTUll _oetection_:imit. (1,') 7)i_
NA -Not analyzed.
1/ -Tentative identification.
~/ -On NROC List of Priority Pollutants.
N. C. Divu.iion o 6 He.a,Uh SVLvicv..
D11S 3068-0 (4/86 Labo11.ato11.y)
BASE/NEUTRAL ANO AC IO
EXTRACT ABLES
COHPO.JNO
nvrene
benzidine
butvl benzvl ohthalate
benz{a)anthracene
chrvsene
3.3-<iichlorobenzidine
bi sf2-<ethvl hexvl J ohtha 1 ate
di-n-octvl ohthalate
benzo{blfluoranthene
benzo(klfluoranthene
benzo(alnvrene
i ndeno ( 1 2. 3-cd) nvrene
dibenzo(a h)anthracene
benzo(q.h il=rvlene
ani 1i ne
benzoic acid
benzvl alcohol
4-chloroaniline
dibenzofuran
2-<rethv 1 ~"'-tha 1 ene
2-<rethvlohenol
4-<nethvloheool
2-nitroaniline
3-nitroaniline
4-nitroaniline
2.4.5-trichlo~henol
J -Estimated value.
• •
STATE LA80RATOOY Of PUBLIC HEALTH
DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUMN RESCIJRCES
P.O. BOX 28041 -306 N. WILMINGTON, SI., RALEIGH, N.C. 21611
OOGANIC CHEMICAL ANALYSIS
LAB NO -1 D 3,;/,;). L/ 70. ',,;i.;i,c;
FIELD# 3 f?[g·z_ ~.fb3
TYPE ( 3) ( ,-3 ) ( . . ) ( l
UNITS =t:1 <ua/ka ·un/Cl tua/ka .. n/1 .. n/ka ua/1 ua/kq
IO/:Hn u__ ,,-----
l,;n/11.S0
101 :1:,o /(lo\-\
/ • ..
. ' I .so, ~L. ,,,, I
J,i/ '130 ,
IO/s~O ~ so,.~ \~
'\O. _.,
~-I ~:v~
I , ' / ' /
<'a , .. ,< l,L LL-.,,
1n1ao
~:,
S"o/Jt,,,:;o
,, ', ,/
m1H-
H2.0I Soll.
to be less than value given.
( ) { l
ua/1 ua/kq "q/1 un/ka
..
,1:.1 VC/J " \.
, \
.,J..'J <;/'!('I( . z
l:!
G,
---~"ND . ,-,
RANCH ,.+
...• r.~\1/
K -Actual value is known
L -Actual value is known
U -l'\aterial was analyzed
NA -Not analyzed.
to be greater than value given.
for but not detected. The nuit>er 1s the Ninirrun Detection Limit.
l/ -Tentative identification.
~/ -On NROC List of Priority Pollutants.
N .C. D-lv-l-6-lon 06 lfc.aU.'1 Sviv-{e,~,~
D/IS 3068-0 [4/56 l.abo1taJ.01u1)
f'VRGEASLE {))Ml'OJHOS
a:JMl>OONO
ch 1orcrnethane
brO'TOT'ethane
dichlorodifluorcmethane
vinvl chloride
chloroethane
methvlene chloride
trichlorofluoranethane
ethene. 1 1-dichloro
ethane I 1-dichloro-
1 2-trans--di ch loroethene
chloroform
ethane 1 2-dichloro-
ethane. 1. l. 1-trichloro-
carbontetrachloride
broiodichlorcmethane
nrnnane. 1.2-dichloro-
l .3-trans-dichlo, ne
trichloroethvlene
chlorodibrcxrcmethane
benzene
ethane 1 1 2-trichloro-
1 3-<:is-dichlo ne
2-chloroethvl vinvl ether
brorofonn
ethane. 1. 1 2 2-tetrachloro-
ethene tetrach loro-
toluene
ch lorobenzene
ethvlbenzene
acetone
2-butanone
carbondisulfide
2-hexanone
4-<rethvl-2~ntanone
stvrene
vinvl acetate
xvl ene.s i+d-a/)
J -Estimated value.
• •
STATE LAllOHATOOY Of f'VBL!C HEALTH
O[V[S!ON Of HEALTH SERV!CES, N.C. OEPARTMENI Of lfJMAN RESOORCES
P.O. BOX 28047 .. 306 N. W!LMINGION, ST., HALEIGH, N.C. 27611
OOGNIIC CHEMICAL ANALYSIS
LAB NO 7/J ::S"'"''_I_ 7('.)~ . ..,...,....,
FIELD#
( 3 ) ·-( 3 ) ( ). ) TYPE
UNITS HO/ I ruo/kn .. nfl ,..,;;/ka .. n/ 1 .. n/ka Hn/1 ua/ka
,/1 / j I I
10 . I, , l,
C-t:.J I Pl (.;..) "1,-(+'J-:IL .,,,
10 I 1 T1 / .
,0 /
< .,,
,o :f .,
0
~~ \.,_,, SI
'1'1.1'; ·-..:...-
,
10 ,-
/ '
JO I,( I'
/o
,;-
/0
/t}
(-
Jo I
~ ,I/ "
MA/)L
... l{I
I I I/,
K -Actual value is kllOWn to be less than value given.
L -Actual value· is known to be greater than value given.
( ) ( l
un/1 un/kn ,on/ 1 un/ka
f'Lllo .. ----...
,, •(JJ '-
\.
\
_,.,,_, <:"IV"it' . z
~
1,/J
PERFUND ">"'l
-" l'l
.... ,AG~
U -Material was analyzed for but not detected. The nUTDer is the Minimu11 Detection Limit.
NA -Not analyzed.
11-Tentativeidentification 4 .~A Ln_ {) J __ J___ +--:-· /
~I -On NROC List of Priorit/Pollutants. fer~ c..X-.-lCl'.T Cvr~a,-u .
N.C. Division of Health Services
IJIIS 30(,8--0 (4/86 l.,1bor.1to1·y)
• •
23 February 1988
To: File
From: Jack Butler
Re: Channel Master, NCD122263825
On this date Ms. Jessica Lau, Tech Law, Inc., visited our office to
review the files for the Channel Master site in Oxford, N.C. Ms. Law is
preparing a report under contract with the U.S. EPA. Ms. Law and I also
discussed the present clean-up of the lagoon area by Channel Master.
JB/pb/O543.27
•
27 January 1988
To: Lee Crosby
From: Jack Butler
Re: Sampling visit to Channel Master
NCD177763825
•
On Jan. 25, 1988, Jack Butler, N.C. CERCLA Unit, visited the Channel
Master site in Oxford, N.C. The purpose of this visit was to collect soil
samples from the bottom of quadrants I and II of the excavated lagoon.
Sampling was performed by Southern Testing under contract with Channel
Master. Laboratory results are pending.
JB/pb/O517b.42
• •
26 January 1988
To: File
From: Jack Butler
Re: Telephone conversation with Giezelle Bennett, U.S. EPA (404-347-3402)
about Channel Master, NCD122263825
Ms. Bennett was contacted on this date to determine her needs on the
subject site. She does not have the file at this time but said that she and
Al Hankey were coming up to visit and discuss this site on Feb. 9, 1988. She
will look at our files and get copies of documents that she needs at that time.
JB/pb/0489b.31
TO:
FROM:
SUBJECT:
• •
20 January 1988
File
Jack Butler
Telephone conversation with Roger Coats (919-934-9711) about
Channel Master, NCD122263825
Mr. Coats was contacted on this date to get an update on activity at
the subject site. Mr. Coats reported that quadrants 3 and 4 of the lagoon
have been filled and that quadrants 1 and 2 have been excavated and are ready
to be sampled as soon as the weather clears. Mr. Coats also informed me that
this facility had been bought by Avnet and that Time Electronics is presently
occupying part of the building. Two other companies are also to occupy this
building in the future. All three of these operations are to be electronic
part distribution centers with no manufacturing activity.
JB/ds/0526b-66
1'. C. Dcpartrrtent of l·ruman Resources •
-Divisir;n of Health Services . ' . SAMPLE ANALYSES REQ.T.
State Laboratory orPublic Health
P. 0. Box 28047
306 N. Wilmington Street
Site Num~r 3 o/ tf) / Z-2 2 6 3 Sf 1,. ~ R.Jcigh, 27611
Field Sample ~umber ~J"--'-J_:Z--;f ___________ _
NameofSite Cfu-,nn@/ Masf"e,-Sitcl.oca:ion Oxrorol,A/,C,
Collected By ::r, (8.,,, 7 /er ID#_¥_,_~---Date Collected / c;, -,,2 7 -? 7
Type of Sample:
Environmental
__ ·_Groundwater (1)
__ Surface Water (2)
_L Soil (3)
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
Comment&
o-3 11
""/
INORGANIC
Extractables
Parameter
__ Arsenic
--Barium
_·_Cadmium
__ Chromium
__ . Lead
__ Mercury
, -~kl'!i'!!." ___ ·
Results mg/1 Parameter
__ Arsenic
__ Barium
__ Cadmium
__ Chloride
__ Chromium
_Copper
__ Fluoride
etcr
__ sulfates
_Zinc
_Ph
__ Conductivity _______ . __ ms
-TOC
__ Silver ---~---· _·_Iron
-· -------------
Parameter Results mg/1
✓ P&T:GC/MS :Z Acid:B/N Ext.
_TOX
--. --
_Lead
_._Manganese
__ Mercury
__ Nitrate
__ Selenium
ORGANIC CHEMISTRY
Parameter Results mg/1
·_EDB .
__ PCB's
__ Petroleum
__ Endrin
· __ Lindanc
Parameter
__ Methoxychlor
__ Toxaphcnc
-2,4-D
__ 2,4,5-TP (silvcx)
--
Time I t>,'/ S'
Rcaulta mg/1
Results mg/1
MICROBIOLOGY RADIOCHEMISTRY
. Parameter Parameter Results PCi/ 1
__ (MF) Coliform Colonics/lOOmls __ Gross Alpha
__ (MPN) Coliform Colonics/lOOmls __ Gross Beta
----
----
DateReccived /().-JJ-f7/3fJ DateRcported l).-J~-rf7
. \ \ '::/'Is-, ~ W (lf' . !31;' H
Date Extracted_;__-..::..·_..;.,,, __________ -"-___ . Date Analy-.<:d , 1. J7-V7 ,1,ur 11-·2,,,.,_. !?] 13(0
/1 d_ . Al /1 J?✓, / ""'0'.~892
Reported Bv (~/71 c<. :-/if"{/\___-Lab Number ____ lfe....:=:.==.c::... _________ J
[)HS 3191 (Re-vised 7185)
SoliJ anJ Ha:.ardow Wane (Rr\·ic-w i 187)
K C. Department of Human Resources • , A,..
-Divisic,n of Health Services . SAMPLE ANALYSES REQ"9 ,._ State laboratory of Public Health
P. 0. Box 28047
306 N. Wilnungton Street
_Raleigh, 276 I 1
Site Number =3~o/.-'--=dJ~/~Z."'-"2=-e2,.._b'---=3~5/'.~1,"--'~"-------Field Sample N~ber ~3"-'-1-'-.J,._j-~ __________ _
Name of Site -'C'-'fz...,___,.,,ZLn'-'n'-'-"@c..L..l--'/"1'--'-"'=s.,_i:;_.,"?-,_c_______ Site Lo=ion O JC-/' 0 ,,-ol, A/, C,
Collected By _::T._, _<8._-w_7,'-'-/e'--'-r ____ ID#_¥_,_~---Date Collected / O -,.2 7 -f17 Time IO,' Jc?
T ypc of Sample:
Environmental Concentrate Comments
__ ·_Groundwater (1)
__ Surface Water (2)
~ Soil (3)
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
,:;::;--5 ,, Com,Pf?'.s,'/-e. :r;c 2 •
__ Other (4)
INORGANIC CHEMISTRY
Extractables Total
Parameter Resulumg/1 Parameter Rcsulumg/1 Parameter
__ Arsenic __ Arsenic __ silver
__ Barium __ Barium __ sulfates
_·_Cadmium _Cadmium _Zinc
-. _ Chromium __ Chloride _Ph
_Lead __ Chromium __ Conductivity
__ Mercury __ .Copper _ms
-~l~11i'!!'l ___ · __ Fluoride _Toe ..
--:Silver -·-lron --
--_Lead --
--_· _Manganese --
-·-__ Mercury --' __ Nitrate_ ----
--__ Selenium --·
ORGANIC CHEMISTRY
Parameter Resulumg/1 Parameter Results mg/ 1 Parameter
±._P&T:GC/MS ·_EDB __ Methoxychlor
Acid: BIN Ext. _·_PCB's __ Toxaphcne
_TOX __ Petroleum _2,4-0
--__ Endrin __ 2,4,5-TP (silvcx)
--__ Lindane --
MICROBIOLOGY RADIOCHEMISTRY
~ulumg/1
Resulumg/1
Parameter Paranieter Results PCi/1
__ (MF) Coliform Colonics/lOOmls __ Gross Alpha
__ (MPN) Coliform Colonies/lOOmls __ Gross Beta
----
-----
(()~ J-7·· v7 .LJ '0
Dare Receiv~d ---~-~6--~'0-"-'~------~-Dare Reported-,;:;::--;------;;--;---;;;~-------
' p,--. 6,1//7
Date Extracted ....,_11;...-S-=··'--.. <-":,s-']__,_P-'-kl=--------~---· Date Analr.cd ii-I '7. <:'c 7 .,.,, u · I I-7--0 -'17 i3 ,0
Reported Bv _______________ Lab Number ?Q'.~8:93
l>HS 3191 (R<vi,.cd 7185)
S.ol1J anJ Ha!lrdow Wane (Re\·iew 7187)
K C. Department of Human Resources • TA,..
-Division of Hcalih Services . SAMPLE ANALYSES REQ'...w.a._
State Laboratory of Public Haith
P. 0. Box 28047
306 N. Wilmington Street
!Weigh, 27611
Site Number =3~<:lf~d)~/_Z.~2.~2~6~3~~-J,,.~~~----Field Sample N~ber _J_J_J_C __________ _
Name of Site C.f,gnn9/ /"?a.s'fer-Sirel.oca:ion Oxroro/,A/,C,
Collected By _:T._,_'8._~_7,_/e~r ____ ID#-~~~-✓---Date Collected / O -,2 7 -117
T ypc of Sample:
Environmental
__ · _ Groundwater (1)
__ Surface Water (2)
L_ Soil (3)
__ Other (4)
Extractablea
Concentrate
__ SoUd (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8) . -'-~·.
INORGANIC CHEMISTRY
Parameter Reaulumg/1 Parameter Reanlumg/1
__ Arsenic __ Arsenic
--Barium __ . Barium
_·_Cadmium __ Cadmium
__ Chromium __ Chloride
__ . Lead __ Chromium
__ Mercury _Copper
, ~Selenium __ __ Fluoride
--·Silver _·_Iron
--_Lead
--_._Manganese
-·-__ Mercury
' __ Nitrate ----__ Selenium
ORGANIC CHEMISTRY
Paramet~r Reaulumg/1 Parameter Results mg/1
Commenu
Total
Parameter
__ silver
__ sulfates
_Zinc
_Ph
__ Conductivity
_TDS
-TOC
------------·
Parameter
..
V P&T:GC/MS ·_EDB __ Mcthoxychlor
✓ Acid:B/N Ext. __ PCB's __ Toxaphenc
_TOX __ Petroleum _2,4-D
.
--_Endrin __ 2,4,5--TP (silvcx)
--· __ Lindanc --
Time /O(ff..>
Results mg/1
Reauhamg/1
MICROBIOLOGY
. Parameter
RADIOCHEMISTRY
.
__ (MF) Coliform Colonies/lOOmls
__ (MPN) Coliform Colonics/IOOmls
Date Received /0 -J. 7 -)/ 7 /8/S)
Date Extracted i \ .!"r-V pc:)
Parameter
__ Gross Alpha
--· Gross Beta
Results PCi/1
Date Reported-;;-::::;---:-----==;----------PT (3,-Jf~
. Dare Analr-"d 11·17-517-.,,,,,-ll··'l-0 · Fi'] (3&
Reported By ---------------Lab Number 7(}.:2894
DHS 3191 (Revised 7185}
Sul1J a.nJ Ha~rdous Wane (Review 7187)
I
K C. Department of Human Resources •
~Divisfrm of HeaJih Services . SAMPLE ANALYSES REQ•T·
Sutc Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh. 27611
Sire Number =3_o/~d)~/~Z,~2.=--'2~6°~3~5/'.~1,~~-·---Field SampleN~ber ~3~7~2~7 _________ _
Name of Site _C~6~q=n~n=e~l._~~~-"'~S~~-e=c _______ Site Location O ;c/C'o,rol, A/, C,
Collected By .::r, (/j~ 7 I er ID# _¥~~'---Date Collected / O -;.2 7 -8 7
Type of Sample:
Environmental
__ · _ Groundwater ( 1)
__ Surf.ice Water (2)
~/_SoU(3} .
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
Comment&
dt: / Co,,.,,,,, os/ :fe-I Z. ,.,
"
INORGANIC CHEMISTRY
Extractables Total
Parameter Results mg/1 Parameter Resulumg/1 ' Parameter
--Arsenic __ Ar5enic __ Silver
__ Barium __ Bariwn __ sulfates
_·_Cadmium __ Cadmium --Zinc
__ Chromium __ Chloride ·-Ph
__ . Lead __ Chromium .--Conductivity
__ Mercury __ Copper __ ms
-~l~~il!!.D __ · __ Fluoride __ TQC
--·Silver _·_Iron --
--.. _Lead --
--_·_Mangan~ --
__ Mercury I -·-·, i --
--__ Nitrate. '
__ Selenium
1--
----
!
ORGANIC CHEMISTRY
Parameter Resulumg/1 Parameter Reaulu mg/1 ' I Parameter
_P&T:GC/MS ·_EDB i . ·--Methoxychlor
L Acid:B/N Ext. __ PCB's ; __ Toxaphene
_TOX __ Petroleum ·--2,4-D
.
--_Endrin --2,4,5-TP (silvcx)
--· __ Lindane --
' RADIOCHEMISTRY
Rciulu mg/1
Reaulta mg/1
MICROBIOLOGY
. Parameter Parameter Results PCi/1
__ (MF) Coliform Colonics/lOOmls
__ (MPN) Coliform Colonics/lOOmls
--Gross Alpha
__ Gross Beta
Dare Receiv~d -L/.::;()_-,,,1_7,.._.-..:..!7_7..__.4=:.Q.=--------~-Date Reported -;;=--:------:::,7.,,..--------
) (I, 6tJJf
Date Extracted -'-11,..:5~. ~-~ITT~~f_<~·~-------~---· Date Analy:cd /l-l>i'-R7 -1,w-. /I· 2,1,'-n @&.
Reported Bv _________________ Lab Nu.-nbcr 70r:!835
DHS JJQJ (R,vi,.,d 7185)
S.ol1J anJ Ha:ardous U/:nu: (Review i/87)
K C. Department of Human Resources •
-Divisi:r,n of Health Services . SAMPLE ANALYSES REQ.T
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611
Sire Number 3o/d) / Z-2 2 63 5(:2,~ Field Sample N~bcr 4J~J_l.-f~-----------
Name of Site .;;C:c..:/2=4!'='1'-'tz"'-"@e...<../---'/"'1~'-'"'=s.,_~_.,,p ... £..J""_______ Site J.,.oca:ion Ox r o ,-o/, A/, C,
Collected By _::r._, _'9._-w_7,_/e ___ r ____ ID#-~~~---Date Collected / 17 -,2 7 -f/7
Type of Sample:
Environmental Concentrate Comment&
__ · -Groundwater (1)
__ Surface Water (2)
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
~ z ct?f1r£t7s/(e. / .Z, 'I ;
_L_ Soil (3)
__ Other (4)
Extractablcs
Parameter Rcsult&mg/1
__ Arsenic
--Barium
_·_Cadmium
-. _ Chromium
__ . Lead
__ Mercury
-~kf!IU.!!1_ -.
__ Silver
-----·-. ·:. --.. --
Parameter Rcsulumg/1
✓ P&T:GC/MS .J.... Acid:B/N Ext.
_TOX
----
MICROBIOLOGY
INORGANIC CHEMISTRY
Total
Parameter Results mg/1 Parameter
__ Arsenic __ silver
__ Bariwn __ sulfates
_Cadmium
. _Zinc
__ Chloride _Ph
__ Chromium __ Conductivity
__ Copper _ms
__ Fluoride _TOC
· _·_Iron --
_Lead --
_·_Mangan~ --
__ Mercury --
__ Nittate. --
__ Selenium --·
ORGANIC CHEMISTRY
Parameter Results mg/1 Parameter
·_EDB --Methoxychlor
_·_PCB's __ Toxaphene
_Petroleum _2,4-D
__ Endrin __ 2,4,5-TP (silvcx)
· __ Lindane --
RADIOCHEMISTRY
Results mg/1
Results mg/1
. Parameter Parameter Rcsulu PCi/ 1
__ (MF) Coliform Colonics/lOOmls __ Gross Alpha
__ (MPN) Coliform Colonics/lOOmls --· Gross Beta
----
-----
Date Receiv~d _,._/;:.O_-_J......;7:...·_-..:oJl_7:......cl'3..:.'&.=c.. ______ ~_ Date Reported -:;;::;c;:--;-----:::-:-;;;---------o' . ~ ~~
DareExrracred 11.C:,-~7 rLL.I .DareAnaly:ed 11-1'?#17~,,,,-11-7---c,,[[7 /!J&
Reported Bv
[>HS }JQJ (R<Viscd 7185)
Sul1J anJ Ha:ardous W.stc (Review 7187)
~-C. Department o( Hu~n Resources •
Di\·isien of Health Services . SAMPLE ANALYSES REQ.T
State Laboratory of PubUc Health
P. 0. Box 28047
306 N. Wilmington Street
Site Number
Raleigh, 27611
=3~o/.~'t0~/_Z~Z~Z~6~3~5(~1,---"S"_· --,--Field Sample ~umber _1_t_z_cr _________ _
Name of Site C fzqnne/
Collected By ::r, ([J,,_, 7 /er
Type of Sample:
Environmental
__ Groundwater (1)
--Surface Water (2)
1 Soil (3) '
__ Other (4)
Extractables
Site J.,oca:ion OX ro>'o/, A/, C,
-~---Date Collected / O -,2 7 -F7
Concentrate · .
__ Solid (5)
__ Liquid (6)
_._ Sludge (7)
__ Other (8)
./
INORGANIC CHEMISTRY
Comment&
Total
Parameter Resulumg/1 Parameter Resulumg/1 Parameter
--Arsenic __ Arsenic __ silver
__ Barium __ Barium __ sulfates
_·_Cadmium __ Cadmium _Zinc
___ Chromium __ Chloride _Ph
-·Lead __ Chromium· __ Conductivity
__ Mercury _Copper _ms
~ --~1~.~i.~~-· . __ -Fluoride _Toe
__ -Silver · _·_Iron --
--_Lead --
--__ Manganese --
-·-__ Mercury --,. __ Nitrate. ----.. --__ Selenium ---
'
ORGANIC CHEMISTRY
Parameter Results mg/1 Parameter Results mg/1 Parameter
./p&T:GC/MS ·-EDB __ Methoxychlor
/ Acid:B/N Ext. _·_PCB's __ Toxaphcne
_TOX __ Petroleum _2,4-D
--__ Endrin --2,4,5-TP (silvcx)
--· _· _Lindane --
Time/,' IS'
a.;.;ults m.g/1
Reaulta mg/1
MICROBIOLOGY RADIOCHEMISTRY
. Parameter . ' Parameter Results PCi/ 1
__ (MF) Coliform Colonics/lOOmls __ G,-oss Alpha
__ (MPN) Coliform Colonics/lOOmls ___ G,-oss Beta
----
----
/ 0 •• ;)._ 7--(/7 di)
Date Recciv~d --'-----'--"~-'---,-'co'--,----'------Date Reported -;;'.::::;,----;-------;::--:--::;---------
. Date Extracted Jj-'J-1/f fii.~. • Date Analy-.<:d r;r;'i/'~ -rwr /8;.) 11--i-,o ·',{,I':>&
J-, 13, ,-,o ,_
---------------Lab Number -----~"-_u_r,;.c..·-=8'-"'9::;..7_,__ __ :-----Reported Bv
[>HS }JQJ (R<ViKd 7185)
S..,l1J anJ Ha:3rdous Wane (R~icw 7187)
KC. Dcpartmc:nt of Human Resources •
,Divisiiln of Hca!th Services . •
State Laboratory of Public Healch
SAMPLE ANALYSES REQ! T . P. o. Sox 28047
306 N. Wilmington Street
Raleigh, 27611
Site Number 3 o/ d:) / Z Z 2 6 3 5/: Z. ~ Field Sample ~.,;,,ber3 ~-7_.J_O __________ _
Name of Site C fzgnn,;,/ /'?a.sfec Site Lo=ion Ox-roro/,A/,C,
Collected By :::r, <8.w7/er ID#_¥~~-'---Date Collected /0-.2 7 -l17 Time /,'Jo
Type of Sample:
Environmental
__ · _ Groundwater (1)
--Surface Water (2)
__L Soil ( 3}
__ Other (4)
Concentrate
__ Solid (5}
__ Liquid (6)
__ Sludge (7)
__ Other (8)
INORGANIC CHEMISTRY
Extrac:tablcs
Parameter Results mg/1
--Arsenic __ Barium
_·_Cadmium
-. _Chromium
__ . Lead
__ Mercury
~l~'!iu.rn __ ·
__ Silver
----
-·-' --. --
Parameter Rcsulumg/1
V P&T:GC/MS
..L Acid:B/N Ext.
_TOX
----
MICROBIOLOGY
Parameter
__ (MF) Coliform Colonics/lOOmls
__ (MPN) Coliform Colonics/lOOmls
Parameter Results mg/1
__ Arsenic
__ Barium
__ Cadmium
__ Chloride
__ Chromium
__ Copper
__ Fluoride ..
· _·_Iron
_Lead
_._Manganese
__ Mercury
__ Nitrate.
__ Selenium
ORGANIC CHEMISTRY
Parameter
·_EDB
__ PCB's
__ Petroleum
__ Endrin
· __ Lindanc
Results mg/ 1
.
Parameter
--Gross Alpha
__ Gross Beta
Comments
Total ~-.; !Y. ..
Parameter ..
Results aag/1
__ Silver ..
__ sulfates
__ Zinc
-Ph
__ Conductivity .. _ms
_Toe
------------.
Parameter Results mg/1
__ Methoxychl.:,r
__ Toxaphene
-2,4-D
__ 2,4,5-TP (silvcx)
--
RADIOCHEMISTRY
Results PCi/ 1
Date Recciv~d _,_J_tJ_-_;i._7_,-__.J'_7..._,t$=ill=---------Date Reported 7h:,--;---------:----------
, / ,., ~ 1/, 7', pr .---i (3/J fr
Date Extracted h-L-<LZ M,uJ, ,DateAnaly:ed i/-/R-'? '._,,,,,,---· ·/l•-Ul-Y1 6&
/.--, 'E,
Reported By __________________ Lab Number ·----,-~,;', 'tOr.,2~.,1'18'-f.:'3-ifJN-----,------
[)HS JJQJ (R,vis,d 71B5)
S.ol1J .2,nJ Ha.:.ardow WastC' (RcviC'w 7/87)
K C. Department of Human Resources •
Divisie,;, of He,.lth Ser~ccs . SAMPLE ANALYSES REQ.T
St.ate Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611
Site Number =3_o/.~'d)~_/-'Z,-=c....=2=...,2~&--=3~~~J,,.'--'~~·-· ___ Rdd Sample Number~· ~7_.J~J __________ _
Name of Site ~C'---'!,'-'-'g=n='1u."i'"-"-l-a..~-'-oa<..C..:-s~tJ~-... c-···_"·-----Site Lo=ion Ox -rorol, A/. C,
Collected Bv _:::r._, _<8._~_7,-'-/ e---'-r ____ ID# _· _~..,_~_, ___ Date Collected / O -,2 7 -? 7
Type of Sample:
Environmental
__ Groundwater ( l)
__ Surface Water (2)
__L_ Soil (3)
__ Other (4)
Extractable,
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7f
_ ... _ Other (8)
INORGANIC CHEMISTRY
~:::-:.:
Parameter Resulumg/1 Parameter Resultsmg/1
__ Arsenic __ Arsenic
__ Barium •>T -__ Barium
_·_Cadmium __ Cadmium
__ Chromium __ Chloride
_·Lead __ Chmmium
--Mercury _Copper
-~k!!il!!." __ · __ · Fluoride
--:Silver _·_Iron
--_Lead
--.... _Manganese
-·-__ Mercury ·,. •. __ Nitrate. ----__ Selenium
ORGANIC CHEMISTRY
Parameter Results mg/1 Parameter Resulu mg/1
---5,-P~T:GC/MS ·_EDB
__ PCB's __ Ac1d:B/N Ext.
_TOX __ Perrolcum
--_Endrin
--· __ · Lindane
Comment&
Total ..
Parameter
__ Silver __ sulfares
_Zinc
_Ph
__ Conductivity
_ms
_Toe
------------·
Parameter
__ Methoxychlor
__ Toxaphenc
-2,4-D
__ 2,4,5-TP (silvcx)
--
Time /,, '[J._,,
Results mg/1
Results mg/1
MICROBIOLOGY RADIOCHEMISTRY
. Parameter .. . Parameter Results PCi/ 1
_ (MF) Coliform Colonies/lOOmls __ Gross Alpha
__ (MPN) Coliform Colonies/lOOmls --Gross Beta
. ----
----
/o-~7-f7.8i). Date Received -'---'----'---'-.,-ri,,-----'-----Date Reported;;..,.,_..,=-:---~:::;--;-:::;---------
'1,/.?, r • /8 /J f-1
Date Extracted // -· 9-3' 7 M · ,,J. • Date Analy-..cd -"1/,.-11<"'-'-,?"--'7 ____ --'-/ '-/-_.7.;,:'4"-'-'-'--'\'1...·..1]....1f6~illL.. __
,...,3.
Reported Bv ______________ Lab Number ----';:';;';1(}~.~.t:85:;f)t,· 'i:9'1-----:----
fJHS }191 (R,v;..,d 7185)
5'.,11J anJ Ha:.ardous Waste (Revirw 7187)
K C. Department of Human Resources •
.Oivisif)n of Hc,,Jth Services . SAMPLE ANALYSES REQ.'F"
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
!Weigh, 27611
Site Number .,,.3'--o/.'-''t0=-.:.../-=2,~2:::...,,,2......:::t:...:3=<---<5/'...._Z.=-S--:,,__· ___ Field Sample Number ...;J;,.._7_:>_2.---__________ _
Name of Site -=C==--=lz=9=n,..;z=@e.l,__--'n'-'C.:""=S.,_f;_.E.._,._c_______ Site J..ocarion Ox -/'orol, A/. C,
Collected By .::r, <8~7/er ID#_¥,_~---Date Collected / o-..2 7 ' 117
Type of Sample:
Environmental
__ ·_Groundwater (1)
__ Surface Water (2)
_L_ Soil (3) .
__ Other (4)
Extractablea
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
INORGANIC CHEMISTRY
Parameter Results mg/1 Parameter Results mg/1
__ Arsenic __ A,.enic
__ Barium __ Barium
_·_Cadmium _Cadmium
-. _ Chromium __ Chloride
__ . Lead __ Chromium
__ Mercury _.Copper
, __ Sclc.nium __ · __ Fluoride
__ ,Silver __ Iron
--_Lead
--_·_Mangan~
-·-__ Mercury
.. ':. __ Nitrate . --. --__ Selenium
ORGANIC CHEMISTRY
Parameter Reaulu mg/1 Parameter Result& mg/ 1
-✓ P&T:GC/MS ·-EDB
:::z'. Acid:B/N Ext. __ PCB's
_TOX __ Petroleum
--__ Endrin
--· __ Lindane
Comments
Totd ---
ParamctJCr
·_._Silver
· __ Sulfates
·_· _Zinc -..
. _Ph
__ Conduaivity , __ ms
. __ TQC
--------
--·
Parameter
. __ Methoxychlor
__ .Toxaphcne
·-Z.4-D
,--2,4,5-TP (&ilvcx)
:
i
Tune Z/170
Results mg/1
Results mg/1
MICROBIOLOGY RADIOCHEMISTRY
. Parameter
__ (MF) Coliform Colonics/lOOmls
__ (MPN) Coliform Colonics/lOOmls
Parameter
__ Gross Alpha
__ . Gross Beta
RcsultsPCi/1
Date Recciv~d /0-;l. 7-rf'.7 IS;J)_ Date Reportcd-;::::---:------;;-;-::;;---------
<7 1/, l'. . fT . l',JJ fl . ?
Dare Extracted ~(<../L-__.9c._-,..tLL.L'.1_.;..M.:..:.;;•(J.)c...;..' ------'----. Date Analy-.cd 11-/P.->?7 ·flJ/ r / / , vl'-)i J fo ~
L,/3.
----------------Lab Number ?O,'ZS;QQ Reported Bv
[)HS }IOI (R,vi,,d 7185)
Sol1J ;;inJ Ha:.ardous \t-'aste (Review 7 /87)
• DIVISION OF liEALTrl SERVICES
SO. AND HAZARDOUS WASTE MANAG,RANCH
Chain of Custody Record
Hazardous Waste Materials
Location of Sampling: Generator
Storage Facility
../ Other: ce A CLA
Company's Name C,4,,,.~ne//'fqJTe-;--
Address a'.x ;,<;.,_..p;t1 , µ c:;. ,
)
Collector's Name~~
,,;> signature
Date Sampled /O-z_'7-T7
__ Transporter _. _Treatment Facility
__ Disposal Facility _Landfill
Telephone( __ ~) _______ _
Tele_phone( ~/ 'r ) 7J 5-2-K"C>/ .
T:ilne Sampled~---------
Type of Process Generating Wastefa~/ rf'lqf,/1.'f ' "-'--'---'-----./+---------------
. Field Information
·Field Sample No. J72.~ J.7Z-,(: f7Zi5' J7Z7 37:z.,,? ..J7Z-? 37JcJ
.373 I J 732.
Chain of Possession:
1. /~L¢:'. ~--:-~/=:....0,,...:-J-"-'--7--='ii:...:..7_ ---U-title I!!/' •. inclusive dates v~nature
2. QA'}I?~ 7 signature inclusive dates •
3. uJ,fi<-~ )Qe.,l}t~i
signature title inclusive dates
Results reported
signature tit.le_ date
Instructions: Complete all applicable information including signatures, and
submit Yith·~nalysis request forms.
SOLID
DIVISION OF EE.ALT!! S:::RVICES
Ah~OUS WASTE !-',A.1'AGEMENT B, Receipt for Samples
The samples described bel01,1 were collected in connection with the adl!linistration,
enforcement, and documentation of the:
( ) North Carolina Hazardous Waste Management Rules, 10 NCAC lOF.
( ) North Carolina Solid Waste Management Rules, 10 NCAC lOG
() Comprehensive Environmental ·Response, Compensation and Liability Act (CERC".i..A)
( ) Toxic Substances Control Act (TSCA). 15 U.S.C. §2601, ~~-• specifically
Sect:ion 11.of TSCA,.15 U.S.C. !l 2610.
Inspector's Name Inspector's Address
Name of Firm Fi'.C!O Address
Finr. ()=er, Ope~·a ~er, or Agent Title
.
•
SAMPLE COLLECTED SAMPLE TYPE,. .. DUPLICATE SAMPLES I SA}'.?LE. LOC.?.TION NUMBER DATE TIME WATER SOIL
Receipt for the sample(s) described.
above is hereby acknowledged:
OTtIER
.
0:FERED
1
ACCEPIED REJECTEDj ON-SITE OIT-S!IE.
I • • •
. . ..
. . ! ·, .
' I I
I
I
Receipt:/rejection of duplicate or split
sai::;,les is hereby 1ecknmdedged·:
. .
Signature of Inspector Sigu1eture of Fi= Q,.,r,er, Operator, or Agent
Title Tit.le
COM!-SNIS, __________________________________________ _
BASE/NEUTRAL ANO ACID
EXTRACT ABLES
COIIPOUNO
N-nitrasodimethvlamine
bis(2 chloroethvllether
2-chlornnhenol
ohenol
1.3-dich lorobenzene
1 4-dichlorobenzene
1.2-dichlorobenzene
bis(2-chloroi llether
hexachloroethane
N-nitroso-di-n~~vlamine
nitrobenzene
isnnhorone
2-nitroohenol
2 4-dimethvlohenol
bis(2-chloroethoxvlmethane
2 4-dichlo~henol
1.2.4-trichlorobenzene
n•nhthalene
hexachlorobutadiene
4-chloro-m-<:resol
hexachlorocvclooentadiene
2 4.6-trichlornnhenol
2-chloronanhthalene
acenaohthvlene
dimethyl ohthalate
2 6-dinitrotoluene
acen•nhthene
2 4-dinitrnnhenol
2,4-dinitrotoluene
4-nitroohenol
fluorene
4-chlornnhenvlohenvlether
diethvl ohthalate
4.6-dinitro-o-cresol
diohenvlamine
azobenzene
4-br~henvlohenvlether
hexachlorobenzene
=ntachlornnhenol
ohenanthrene
anthracene
dibutvl ohthalate
fl uoranthene
J -Estimated value.
• • STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. OEPARTHENT OF HUHAN RESOURCES
P.O. BOX 28047 -306 N. WILHINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEHICAL ANALYSIS
LAB NO 'JC,). :;q z~ ·7az ,,q 2 702-Y<J <l 70?.,i/9..:;
FIELD # ,37,s~-LJ :::i-, .;2.i,-""iP , .. ">,7,>-J
TYPE I.-~ l I 3 l I_:,, l ( 3)
UNITS .. nf.Vua/kn' ,,.,.,,.,/ .. n/ka , .. aLj..l .,n/kQJ .,u,J..V,,aik<1)
~'..\ n /IL .-,.c---
I
• I
IL, ,<;lJ
3.:>.0
I .,,"'D
.13 o
i
..,y
t;.<::7)
I
"11
-.,:;1,-,
:;;:·;i 0
I ,,,-v
33(]
' I ~ I .. ' •I .. '
K -Actual value is known to be less than value given.
7ol,ft 'I/;;
"'I 7d/. f'
( -~)
-...,;..ifuaikri
I'\-
..
L -Actual value is known to be greater than value given.
U -Haterial was analyzed for but not detected. The mnber is theJij_ninun Detection Limit. />17JL..
NA -Not analyzed.
1/ -Tentative identification. £I -On NROC List of Priority Pollutants.
N. C. V,i.v,u.,,i.on 06 He.aLth Sv,.v,i.cv.,
VHS 3068-0 (4/86 LaboJurto~y)
(])
702..lt4 >'1
=?7d-4
( ~)
unL,,-.. nikn"I
BASE/NEUTRAL AND ACID
EXTRACTABLES
aJl1POUND
ovrene
benzidine
butyl benzvl phthalate
benz(alanthracene
chrysene
3 3-<lichlorobenzidine
bis(2...,thvlhexvllnhthalate
di-n-octvl Dhthalate
benzo(b}fluoranthene
benzo(klfluoranthene
benzo(a)nurene
indeno( 1 2.3-cdlnurene
dibenzo(a hlanthracene
benzo(o h.i)nPrvlene
aniline
benzoic acid
benzvl alcohol
4-chloroani 1 ine
dibenzofuran
2-<nethvlnaohthalene
2-<nethvlohenol
4-<nethylphenol
2-nitroani 1 ine
3-nitroani 1 ine
4-ni troani 1 i ne
2.4 5-trichlo~henol
J -Estimated value.
• • STATE LABORATORY Of PUBLIC HEALTH
DIVISION Of HEALTH SERVICES, N.C. DEPAATMENT Of HUMAN RESOURCES P.O. BOX 28041 -306 N. WILMINGTON, SI., RALEIGH, N.C. 21611
ORGANIC CHEMICAL ANALYSIS
LAB NO • .,.,._:} f? q ?. 702-X'l 1 7,, 2-,'Nl 1./ ?:;>.?,X'-1. C
FIELD# ~7,:J. v . "1·7 .. )-~-. ..n;i..£, 37J."7
TYPE ( ~)' ( :,, ) ( '?} ("~ )
UNITS 'uu, 11 uu/kq/ .. uoJ.I /Go/kq) .. , /kq, .,..,;-1 ,fi,/ka) .
-~.'In I,(_. u.., t..L ~
II, ~-V
3.~l)
I ....,.,
)l, '\V
330
=?·::in
Hrro
I
' ,, '/ ..,,. ~/
lt,so !,t... ,. lA. i.L
I
d,
-{~n -I
' ~
I 1,,.(1:J
;
.... '/ '✓ ,,, 'l.r . /
/'>1 l)l ..
(~/2.. SOIL.-
to be less than value given.
70 7 ,--,r ,;
"i·7,.:) .. f(
( :=n . .. /ko .,
',,
I -
' I
K -Actual value is known
L -Actual value is known
U -Material was analyzed
NA -Not analyzed.
to be greater than value given.
for but not detected. The nuri:>er is the MinillUll Detection Limit{YI J)L
1/ -Tentative identification.
~I -On NRDC List of Priority Pollutants.
N, C. D-i.v,{,6-i.on o 6 fie.aU.li Sviv-i.c.e.,;
OHS 3068-0 {4/86 Laba/t.a..ta~y)
---
702-%4"7
~7;;i__q
{ "31
-m>/..1. r.,n/lca) .,
'/
,(_
' ,,
BASE/NEUTRAL AND ACID
EXTRACTABLES
COMPOUND
N-nitrosodimethvlamine
bis(2-chloroethvllether
2-chlornnhenol
ohenol
1.3-dichlorobenzene
1.4-dichlorobenzene
1.2-dichlorobenzene
bis(2-chloroi llether
hexachloroethane
N-nitroso-di-n..nrnnv]amine
nitrobenzene
i snnhorone
2-nitroohenol
2.4-dimethvlohenol
bis(2-chloroethoxvlmethane
2.4-dichlo~henol
1.2.4-trichlorobenzene
n•nhtha 1 ene
hexachlorobutadiene
4-chloro-m-cresol
hexachlorocvclnnPntadiene
2.4.6-trichloroohenol
2-chloronanhthalene
acen•nhthvlene
dimethyl phthalate
2.6-dinitrotoluene
acenaohthene
2.4-dinitrnnhenol
2 4-dinitrotoluene
4-nitrnnhenol
fluorene
4-chlornnhenvlohenvlether
diethvl ohthalate
4.6-dinitro-o-cresol
diohenvlamine
azobenzene
4-bramohenvlphenvlether
hexachlorobenzene
n<>ntachlornnhenol
ohenanthrene
anthracene
dibutvl ohthalate
fl uoranthene
J -Estimated value.
• STATE LABORATORY Of PUBLIC HEAL,
DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 21611
ORGANIC CHEMICAL ANALYSIS
LAB NO "J i};l.fl "t V --, 0·1 Vi~ C. ,o,;)-~ 0 /1
FIELD# 3 '7.::Jo .7. '731 ?>73 &-
TYPE ' 3) ,:.i I 3 l ( )
UNITS -""/-itua/ka) .,,.,.✓,,n/k;') ~•n/-lt'uq/kq) .. n/] un/ka . , ,,.._ '~ ~
l _-
',-)
:,,_~
~
I
I "' '1
)~
'1, ,\
V
'-.
.
• d
.j
I~
;;
\,j "' 'I..
•>.
~ " /
" ,::;,__:r O ~
\ " ,,L
'1( LA-,,
K -Actual value is known to be less than value given.
( l
un/ 1 .. n/ka
L -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. The m1rber is the Mini11U11 Detection Limit. fv17)L
NA -Not analyzed.
1/ -Tentative identification. ii -On NROC List of Priority Pollutants.
N. C. Vj_v,u.,;_on 06 He.aLth SeJtvj_c.v.,
VHS 3068-0 (4/86 LaboJuLto~y)
( l
un/1 un/ka
I
' BASE/NEUTRAL AND ACID
EXTRACTABLES
CXJl1POOND
nurene
benzidine
butvl benzvl nhthalate
benz!alanthracene
chr"sene
3 3-<lichlorobenzidine
bisl2-,,thvlhexvllnhthalate
di-n--octvl nhthalate
benzolblfluoranthene
benzolklfluoranthene
benzo(a)nurene
i ndeno ( 1 2 3---<:d' nurene
dibenzo(a.hlanthracene
benzo(• h i'=rvlene
aniline
benzoic acid
benzvl alcohol
4---<:hloroaniline
dibenzofuran
2-nethvl••nhthalene
2-nethvlohenol
4-nethvlnhenol
2 nitroaniline
3--nitroaniline
4--nitroaniline
2 4.5-trichloroohenol
J -Esti"'3ted value.
• • STATE LABORATORY Of PUBLIC HEALTH
DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOORCES
P.O. BOX 28041 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC ()jEMICAL ANALYSIS
LAB NO '7 (),).. Jf-"l f 70,;\ 519q ?o--,<Joa
FIELD# -~✓~ u -=J·, ,;,, I -'7::?2. . -
TYPE ( 3) L '3 l 3 ) ( l
UNITS _ • .n.l..l✓.,n/k'n'! _.,..,:.~ "'/kq"J 4,0/-I /4/ko'. .. n/1 .. n/ka
,z:::--I/.--~
.
.
.... J
I":\ :,
~
\.
I ... ' . J
y
~
~ IA-IJ u-.
)~
11
<\ .•
'
ti
'V
Cl~
~·{ 'v '✓ 7
Cl ....
" ••
'\ ~
'
K -Actual value is known to be less than value given.
( l
un/1 un/ka
L -Actual value is known to be greater than value given.
U -Material was analyzed for but not detected. The nurrt>er is the Minirrun Detection Limit. /)'1 UL NA -Not analyzed. ---
1/ -Tentative identification.
~I -On NRDC List of Priority Pollutants.
N. C. V-<.v-u-i.on 06 //ealth SVJ.v-i.ei'/2
VHS 3068-0 l4/86 LaboJta.J:o~y)
(!lJ
( )
un/1 un/ko
• • STATE LABORATORY Of PUBLIC HEALTH
DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUHAN RESOURCES
P.O. BOX 28047 -306 N. WILHINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEHICAL ANALYSIS
PURGEABLE CXJHPOUNDS LAB NO 'l I) 1 RC/,., 7()o.''xq,;,, 'IO JRqLJ 7 /J-1 '?4 >:
FIELD#
CXJHPOUND TYPE ( ;,, 1 I 3 1 I 31 ( 3 l
UNITS "n/) /'"1/ka; .. n/ 1 (ijq/kq; ua/l ,-;;;;-/kc( )un/1 ',,,a/ka"'
chlorarethane /0 I l IL
-
.,\_ --Ll
brooonethane /6 I
dichlorodifluoranethane VJ
vinvl chloride JO
chloroethane JO
rrethvlene chloride ~
trichlorofluorarethane z_o I
ethene. 1. 1-<lichloro ~ I
ethane. l. 1-<lichloro-I
1.2-trans-<lichloroethene
chlorofonn
ethane. 1.2-<lichloro--1 I
ethane. 1. 1. 1-trichloro-I
carbontetrachloride
brarodichloranethane
pranane. 1.2-<lichloro-
1.3 trans-<lichlo ne
trichloroethvlene
chlorodibraranethane
benzene I
ethane_ 1 1.2-trichloro-I I I I
l 3-cis-<lichlo, ne I I I
2-chloroethvl vinvl ether Jo I
brarofonn > ~ I
ethane. 1. 1 2-2-tetrachloro-
ethene tetrachloro-
toluene
chlorobenzene , .
ethvlbenzene \ I \ / \ I ' I ' I
acetone JD i, ' j l i,
2---butanone JO I
ca rbond i SU 1f i de -~
2-hexanone JO
4-<rethv1-2~ntanone 10
stvrene ~-
vinvl acetate /0 I
xvlenes Mal) s-,v I I ,J
MfL
,,l-j/✓,
/ V f ,
J -Estunated value.
K -Actual value is known to be less than value given.
L -Actua) value is known to be greater than value given.
U -Hater1al was analyzed for but not detected. The nUTt>er is the Hininun Detection Limit.
NA -Not analyzed.
1/ -Tentative identification. fl -On NRDC List of Priority Pollutants.
N.C. Division of Health Services
DHS 3068-0 (4/86 Laboratory)
70 ~ 'i<Ci I, 70::!'t?CJ '7
C -3 l ..31_
ua/ 1 (/,a/ka <,n/J('.,n/ka'
A J,;__
I
I
\ I I
I A
,,
~ I I
• • STATE LABORATORY Of PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC OlEMICAL ANALYSIS
PURGEASLE COHPOUNDS LAB NO ,..,/\o'ffqg ")cJ;};(GO 7().:1011n
FIELD#
TYPE ( ;:i l ( ?, l ( '3 l ( l COHPOUND UNITS un/1 ,rn7ia: un/ l ,.n/ko, un/ 1 ,•,;;./krl/ .. n/1 un/ko
ch lorcrnethane .0 / l • "---
j_O -braranethane
dichlorodifluorcrnethane · rv
vinvl chloride -0
ch l oroethane 0 I
rrethvlene chloride .) I
trichlorofluoronethane 2-tJ I I
ethene, l 1--<lichloro L,' I I
ethane. l 1--<lichloro--I I I
1,2-trans--<lichloroethene I I
chlorofonn I I
ethane. l 2--<lichloro--I I
ethane. 1-. l. 1-trichloro--I I
carbontetrachloride I I
branodichlorcrnethane I I
orf"'naoe l 2--<lichloro--I I
1.3-trans--<lichlo ne I I
trichloroethvlene I I
chlorodibraranethane I I
benzene I I
ethane, l, 1.2-trichloro--I I I
l 3-cis--<lichlo, ne I
2-chloroethyl vinvl ether /0 I
brorofonn 5 ~I
ethane l l 2 2-tetrachloro--
ethene. tetrachloro--
toluene
chlorobenzene ' ' ethyl benzene . I ' ' '·
acetone Jo I' ~ [A~ I • -
2-butanone JO I I
carbondisul fide '?
2-hexanone JO
4--<rethvl-2...oentanone /iJ
stvrene -~
vinyl acetate JD /
xvlenes Mai) ,.: ' I ' I , I
M ~-
,/1/r
, • ' (I
J -Estimated value.
K -Actual value is known to be less than value given.
L -Actual value· is known to be greater than value given.
u -Material was analyzed for but not detected. The nuroer is the Mininun Detection Limit.
NA -Not analyzed, 1/ -Tentative identification. g1 -On NROC List of Priority Pollutants.
N.C. Division of Health Services
DHS 3068-0 (4/86 Laboratory)
( l ( l
.. ~/1 .. n/ko un/] .. n/ko
,
.,.
•
North Carolina Department of Human Resources
Division of Health Services
P.O. Box 2091 • Raleigh, North Carolina 27602-2091
James G. Martin, Governor
David T. Flaherty, Secretary Ronald H. Levine, M.D., M.P.H.
April 28, 1988
Dr. Mark McClanahan
Agency for Toxic Substances and Disease Registry
Building 30-S Chamblee
1600 Clifton Road, N.E.
Atlanta, Georgia 30333
Lear Dr. McClanahan:
RE: Channel Master N::D122263825
Industrial Drive
Oxford, NC 27565
State Health Director
As --e discussed in our telephone conversation on 25 April 1988, the
following is a brief surmnary of the Channel Master site, NCD122263825.
The Channel !-<.aster site is located on Industrial Drive, Oxford,
Granville County, NC. This facility was constructed in 1962 and used by JFD
Electronics until 1979. JFD was a manufacturer of television reception
antennas. A lagoon was built on the site in about 1964 or 1965 and used to·
dispc se of sludge generated by treating wastewater. The wastewater was
primarily rinse water from a chromate conversion process and ocpper/nickel
electroplating. In 1983 about 50% of the lagoon was backfilled and used as a
truck parking area. The lagoon reportedly held 800 , 000 to 1,000 , 000 gallons
of sludge. During 1986 Channel Master installed 5 permanent ground water
monitoring ~lls (see attachment 1) and performed chemical analysis on the
sludge in the lagoon and soil on the site. Analysis of a compcsite of tbe
sludge sho--ed 99,000 ppm total Chromium, 0.05 ppm extractable Chromium, 320
ppm total Lead and other heavy rretals (see attachment 2). Analysis of water
samples ocllected from on-site monitoring --ells 1 through 4 indicate m
significant chromium contamination in the ground water (see attachments 3 ,4,
and 5). Analysis of core samples from monitoring --ell /IS did mt indicate the
presence of extractable chromium (see attachment 6). Analysis of ground water
from the monitoring --ells did indicate the presence of halogenated
hydrocarbons including trichloroethylene and tetrachloroethylene. further
soil sampling idicated that the halogenated hydrocarbon contamination was part
of a plurre originating near a loading dock on the south side of the main
building.
, ' •
Mr. McClanahan
3-28-88
Page 2
In the early sunnrer of 1987, Channel Master undertook a clean up of the
chromium sludge cxmtamination in the lagoon area. This chromilllll sludge
rerroval is intended to be phase one of a t\o.O part clean up process. Phase t\o.O
is intended to address the halogenated hydrocarbon contamination in the ground
water. Channel Master has now rerroved approximately 14,000 yards3 of
contaminated soil and sludge which has created a pit approximately 20 feet
deep in tre former lagoon area. Sampling of soil from the bottom of this pit
indicates .chromium contamination has been reduced to ro rrore than 300 to 500
ppm total chromium with less than 0.20 pprn extractable chromium.
Contamination levels on the side walls of tre pit are in the range of the
background levels at 10 to 15 ppm total chromium and less than 0 .20 ppm
extractable chromium.
During the past year personnel from the North Carolina CERCLA Branch
prepared and submitted to EPA Region IV a Site Investigation Report and HRS
score for the Channel Master site. This has lead to this site being scheduled
for update 117 of the National Priority List.
As discussed in our telephone conversation on 25 April 1988, Channel
Master and the North Carolina Superfund Branch are seeking ans~rs to the
fo !lowing is Si£S :
1. Can the excavated lagoon be refilled with clean fill dirt from
off site without further excavation, and if rot, what remediation
level for chromilllll in the soil should be sought.
2. If the pit in the lagoon area is filled at this time can the EPA
or ATSDR provide any assurance that a future Remedial
Investigation/Feasibility Study will rot result in a requirement
to reexcavate the pit.
Please respond as soon as possible and thank )DU for :,0ur assistance in
this project. If )DU have any questions, please contact me at (919) 733-280L
JB/ds/0489b.52-53
Sincerely,
~-~_£.L,,,,,/
Jack Butler, Environmental Engineer
Superfund Branch
Solid Waste Management Section
I
I
I
II
•
DJ
I
•
11
-• • • II
II
lW
OJ ;,
-rl
" Q
>,
" w
"' :,
SJ
" H
'--....._
' '
•
Main
Buildi.ng
Southern Railroad
' ' I
Warehouse
LEGEND:
• Monitor Well
C /ff· I _,, C ,;'f-.s'
...-
av,__..::;._,;. ________ T"" ____ M_o_n_it_o_r_w_e_1_1_L_o_c_a_t_io_n_s ___ ...,. ___________ _J
PROJECT IS Channel Master
Oxford, N.C. Ill ·••c.•-·••m ..• , .. ""'"""
I
.... 0, .............. ..
SOIL B MATERIAL ENGINEERS, INC.
RALEIGH, NORTH CAROLINA
Attachment 1
SC ALE: Not to Scale
JOB NO: 055-85-139B
FlG. NO: 2
)
I •
. I G . ~ I Attachment 2 trio Environment o ysts, Inc.
P.O. Oox 12542 • Reseorch Triangle Par<. NC 27709 • 919-467-9919
January 22, 198b
Buddy Mil ls
Channel Haster
P.O. Box 1416
Smithfield, NC 27577
RP-ference: IEA Report No. 350-8
Dear Mr. Mills:
Transmitted herewith are the results of analyses on a single sample submitted · to our laboratory on January 13, 1986. The sludge sample was a composite of the pit from top to bottom. The extraction procedure toxicity was performed on the sludge "as is" (wet weight basis) acc·ording to SW846 Method 1310.
Please see the attached sheet for your results.
Very truly.yours,
INDUSTRIAL & ENVIRONMENTAL ANALYSTS, INC.
~g-~
/;os:ph B. Adamovic
Senior Chemist
JBA/sbm
Enclosure
Offices and loborotories located in: Essex Junction. Vermont
Research Triangle Pork. North Carolina
'
)
•
January 22, 1986
IEA REPORT NO. 350-8
Page 2
Total Arsenic
Total Barium
Total Cadmium
Total Chromium
Tota 1 Lead
Total Mercury
Total Selenium
Total Silver
EP-TOX Arsenic
EP-TOX Barium
EP-TOX Cadmium
EP-TOX Chromium
EP-TOX Lead
EP-TOX Mercury
EP-TOX Selenium
EP-TOX Silver
Results for total metals are reported on a
Sludge Pit
Comp_osite
mg/kg 52.
mg/kg 800
• mg/:,g 20
mg/kg 99,000
mg/kg 320
mg/kg < 0.02
mg/kg 13
mg/kg < 2.5
mg/L < 0.005
mg/L < 0.2
mg/L < 0.01
mg/L 0.05
mg/L < 0.005
mg/L < 0.002
mg/L 0.012
mg/L < 0.05
dry veight basis.
:-
--~
1rtltrial & Environmenta-alysts, Inc.
1---rn P.O. Dax 12542 • Research Triangle Parl<. NC 27709 • 919-467-9919
November 11, 1985
Mr. Buddy Mills
Channel Master
P.O. Box 1416
Smithfield, NC 27577
Reference: IEA Report No. 350-2
Dear Hr. Mills:
JL
Transmitted herewith are the results of analyses on four samples submitted to
our laboratory on October 29, 1985.
Please see the attached sheets for your results.
Very truly yours,
INDUSTRIAL & ENVIRONMENTAL ANALYSTS, lNC.
ft~~
Senior Chemist
JBA/sbm
Enclosure
Offices and loboro1ories located in: Essex Junction. Vermont
Research Triangle Pork. North Carolina
November 11 1 1.
IEA REPORT NO. 350-2
Total Organic
Halide Rep. 1
Total Organic
Halide Rep.2
Total Organic
Halide Rep. 3
Total Organic
Halide Rep.4
Total Organic
Carbon Rep.l
Total Organic
Carbon Rep.2
Tota 1 Orga.nic
Carbon Rep. 3
Total Organic
Carbon Rep.4
pH -
pH
pH -
Rep. l
Rep.2
Rep.3
pH -Rep.4
Specific Conductance
Rep.l
Specific Conductance
Rep.2
Specific Conductance
Rep.3
Specific Conductance
Rep.4
Cadmium
Chromium
Nickel
Copper
pg/L
pg/L
µg/L
µg/L
mg/L
mg/L
mg/L
mg/L
µS/cm
pS/cm
µS/cm
µS/cm
mg/L
mg/L
mg/L
mg/L
< 10
< 10
< 10
12
< 1.0
< 1.0
< 1.0
< 1.0
6.30
6.30
6.30
6.30
134
134
133
134
< 0.01
< 0.03
< 0.03
< 0.02
HWZ
41
41
41
41
3.3
3.3
3.3
3.3
6.70
6.70
6.70
6.70
2030
2040
2030
2000
< 0.01
< 0.03
0.07
< 0.02
HW3
160
160
160
160
25
25
25
25
6.70
6.75
6.75
6. 70
1630
1650
1660
1650
< 0.01
0.08
0.28
0.05
HW4
350
350
350
j50
14
14
14
14
6.50
6.55
6.50
6.50
1560
1570
1570
1560
< 0.01
< 0.03
0.04
0.05
November 11, 1985
!EA REPORT N0-2
Page 2
('1
J ,\
Upstream H\12 H\13 H\14
Arsenic mg/L < 0.005 < 0.005 < 00 0.021
Barium mg/L < 0.2 < 0.2 < 0.2 < 0.2
Lead mg/L < 0.005 < 0.005 < 0.005 < 0.005
Selenium mg/L < 0.005 < 0.005 < 0.005 < 0.005
Silicon mg/L 26 39 29 18
Mercury mg/L < 0.002 < 0.002 < 0.002 < 0.002
, ..
,. ,. a ' '
I
' I
' ~
rn \
1&striol & Environmento.nolysts. Inc. \
P.O. Dox 12542 • f1.eseorch Triongle Pork. NC 27709 • 919-467-9919
November 15, 1985
Hr. Buddy Hills
Channel Master
P.O. Box 1416
Smithfield, NC 27577
f
~
Reference: IEA Report No. 350-3
Dear Mr. Mills:
Transmitted herewith are the results of analyses on four samples submitted to
our laboratory on November 6, 1985.
Please see the attached sheets for your results.
Very truly yours,
INDUSTRIAL & ENVIRONHENTAL ANALYSTS, INC.
~~a~c:2f::;.ovic~~---z:.______.-f ~:nior Chemist
JBA/sbm
Enclosures
Offices and loborotor1es located in: Essex Junction. Vermont
f\eseorch Trrongle Pork. Nonh Carolina
November 15, 198. • IEA REPORT NO. 350-3
MLJ,\
Opstream HW2 HWJ HW4
Total Organic
Halide Rep. l µg/L 11 57 130 350
Total Organic
Halide Rep.2 µg/L 10 56 130 340
Total Organic
Halide Rep.J µg/L 11 57 130 340
Total Organic
Halide Rep.4 µg/L 11 56 130 340
T.-,t;,J Or3anic
Carbon Rep. l mg/L < 1.0 6.5 13 22
Total Organic
Carbon Rep.2 mg/L < 1.0 6.5 13 22
Total Organic
Carbon Rep.3 mg/L < 1.0 6.5 13 22
Total Organic
Carbon Rep.4 mg/L < I. 0 6.5 13 22
pl! -Rep. l 5.80 6.60 6.60 6.50
pH -Rep. 2 5.90 6.65 6.60 6.55
pH -Rep. 3 5.85 6.60 6.60 6.60
I pH -Rep.4 5.90 6.60 6.60 6.60
Specific Conductance
I Rep. 1 µS/cm 137 1990 1650 1560 " I Spec i fie Conductance
I Rep. 2 pS/.::m 136 2020 1680 1540 I I Specific Conductance
I Rep.3 pS/cm 135 2020 1650 1580 ,, I .
(, Specific ConductcJncc
~ ! Rep.4 11S/cm 136 1970 1680 1550 .,
,t
} I Cadmium mg/L < 0.01 < 0.01 < 0.01 < 0.01
'if, t Chromium mg/L < 0.03 < 0.03 < 0.03 < 0.03 ' 'i: • ' Nickel mg/L < 0.03 0.04 0. 19 < 0.03 (;,)
Copper mg/L < 0.02 < 0. 02 < 0.02 0.02 .j •
I
• ~
November is, 19;tt
IEA REPORT NO. 3 -2 • Page 2 ~~0 /\
Upstream MW2 MW3 MW4
Arsenic mg/L < 0.005 < 0.005 < 0.005 < 0.005
Barium mg/L < o. 2 < 0.2 < 0.2 < 0.2
Lead mg/L 0.006 < 0.005 < 0.005 < 0.005
Selenium mg/L < 0.005 < 0.005 < 0.005 < 0.005
'j·
Silicon r.ig/L 24 37 28 9.8
Mercury mg/L < 0.002 < 0.002 < 0.002 < 0.002
I ,
~· I
~ I
• ,I
·I
I
ii
Ii
I!
I
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r
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< ' ·, " ;, . -
:--
: -
-:,a
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II
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11
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~
I.trial & Environment.olysts, Inc. r l rn P.O. Oox 12542 • Research Triangle Porl<. NC 27709 • 919-467-9919
November 22, 1985
Mr. Buddy Mi 11s
Channel Master
P.O. Box 1416
Smithfield, NC 27577
Reference: IEA Report No. 350-5
Dear Mr. Mi 11s:
Transmitted herewith are the results of analyses on four samples submitted to
our laboratory on November 13, 1985 .
Please see the attached sheets for your results.
Very truly yours,
INDUSTRIAL & ENVIRONMENTAL ANALYSTS, INC.
~t~ovic /~:;~~~ ~~emist
JBA/sbm
Enclosures
Offices and loboromr,cs locrned 1f"l: Essex Junction. Vermont
Research Triangle Pork. North Carolina
J
November 2Q, 1985 -
!EA REPORT NO. 35 -/})l,4)·-1
Upstream ffi/2 ffi/3 ffi/4
Total Organic
.Halide Rep.I µg/L 16 160 210 340
I Total Organic
Halide Rep.2 µg/L 16 150 210 340
I Total Organic
Halide Rep.3 µg/L 15 150 210 340
II Total Organic
Halide Rep.4 µg/L 15 150 210 340
(1 I Total Organic
Carbon Rep.l mg/L < 1.0 6.5 13 22
I! I Total Organic
~ Carbon Rep.2 mg/L < 1.0 6.5 13 22
• Total Organic
i Carbon Rep.3 rng/L < 1.0 6.5 13 22 ,,
• Total Organic
Carbon Rep.4 mg/L < 1.0 6.5 13 22
i pH -Rep. 1 6.07 6.53 6.40 6.64 -pH -Rep. 2 6.06 6.63 6.47 6.66
i Rcp.3 6.08 6.65 • pH -6.51 6.74
pH -Rep.4 6.10 6. 70 6.40 6.75 ! • Specific Conductance
Rep. 1 uS/cm 139 2000 1600 1700
• Specific Conductance
Rep.2 µS/cm 139 1990 1610 1700
Ii Specific Conductance
Rep.3 µ5/cm 138 2020 1590 1690
Specific Conductance • Rep.4 µS/cm 139 2010 1610 I 710
Cadmium mg/L < 0.01 < 0.01 < 0.01 < 0.01
II Chromium mg/L < 0.03 < 0.03 0.04 < 0.03
-Nickel mg/L < 0.03 0. 01, 0. 15 < 0.03
Copper mg/L < 0.02 < 0.02 < 0.02 0.02
fl
&!
·-
___,.
'
November 22, 1-
IEA REPORT NO. 5 • Page 2
I rY)(A)-/
Upstream HW2 HW3 HW4
I Arsenic
Barium
mg/L < 0.005 < 0.005 < 0.005 < 0.005
mg/L < 0.2 < 0.2 < 0.2 < 0.2
I Lead
ti Selenium
mg/L < 0.005 < 0.005 < 0.005 < 0.005
mg/L < 0.005 < 0.005 < 0.005 < 0.005
' • Silicon mg/L 24 37 30 16
"
~ II Mercury
I ;·
mg/L < 0.002 < 0.002 < 0.002 < 0.002
•
Ii
•
II
• -!
II
I
ti
! ' •
ti
fl
II
I t
I
r··
1eustriol & Environment.nolysts, Inc.!
P.O. [lox 12542 • Research Triangle Porl,, NC 27709 • 919-467-9919
March 20, 1986
Felix Killette
Channel Master Co.
P.O. Box 1416
Smithfield, NC 23994
Reference, IEA Report No. 115-46
Dear Mr. Killette,
Transmitted herewith are the results of analyses on eight samples submitted
to our laboratory on March 6, 1986.
The extraction procedure toxicity was performed according to SW846 Method 1310.
Please see the attached reports for your results.
Very truly yours,
INDUSTRIAL & ENVIRONMENTAL ANALYSTS, INC.
fa-ilij_~~
,./ Joseph B. Adamovic t ·
Senior Chemist
JBA/sbm
Enclosures
:;1/( {u
<f' C0te..
Offices and laboratories located in, Essex Junction. Vermont
Research Triangle Pork. North Carolina
.. • •
) VOLATILE FRACTION
CLIENT SAMPLE NO. MW-5
IEA SAMPLE NO. 115-46-9
NUMBER COMPOUND DETECTION CONCENTRATION
LIMIT (µg/L) (µg/L)
1 ACROLEIN 300 BDL*
2 ACRYLONITRILE 300 BDL
3 BENZENE 30 BDL
4 BROMODICHLOROMETHANE 30 BDL
5 BROMOFORM 30 BDL
6 BROMOMETHANE 30 BDL
7 CARBON TETRACHLORIDE 30 BDL
8 CHLOROBENZENE 30 BDL
9 CHLO ROE THANE 30 BDL
10 2-CHLOROETHYVINYL ETHER 30 BDL
11 CHLOROFORM 30 BDL
12 CHLO ROME THANE 30 BDL
13 DIBROMOCHLOROMETHANE 30 BDL
14 1,2-DICHLOROBENZENE 30 BDL ,) 15 1,3-DICHLOROBENZENE 30 BDL
16 1,4-DICHLOROBENZENE 30 BDL
17 1,1-DICHLOROETHANE 30 BDL
18 1,2-DICHLOROETHANE 30 BDL
19 1,1-DICHLOROETHENE 30 BDL
20 trans-1,2-DICHLOROETHENE 30 BDL
21 1,2-DICHLOROPROPANE 30 BDL
22 cis-1,3-DICHLOROPROPENE 30 BDL
23 trans-1,3-DICHLOROPROPENE 30 BDL
24 ETHYL BENZENE 30 BDL
25 METHYLENE CHLORIDE 30 BDL
26 1,1,2,2-TETRACHLOROETHANE 30 BDL
27 TETRACHLOBQETHENE 30 950.
28 TOLUENE 30 30.
29 1,1,1-TRICHLOROETHAHE 30 BDL
30 1,1,2-TRICHLOROETHArrE 30 BDL
31 IJlICHI OROEIHEe!E 30 7000.
32 TRICHLOROFLUOROMETHA~ 30 BDL
33 VINYL CHLORIDE 30 BDL
*BDL -Below Detection Limit
Sample diluted by 5 due to a high concentration of trichloroethane.
--
,.
March 20, 1986
IEA Report No. 115-46
MW-5 MW-5 MW-5 MW-5 MW-5 MW-5 MW-5 MW-5
Core, S&>Mtf'le, o1.tPfJ.s (ffJ-,19. 5-21. 0 23.5-24.8 26.0-27.5 28.5-30.0 33.5-34.4 38.5-38.9 43.5-43.8 53.5-55.0
EP-TOX Arsenic mg/L < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 NO < 0.00-
EP-TOX Barium mg/L < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 ------< 0.2
...
EP-TOX Cadmium--. mg/L < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 ------< 0.01
EP-TOX Chromium '.mg/L .. -< 0.03 < 0.03 < 0.03 < 0.03 < 0.03 < 0.03 ------< 0.03
EP-TOX Lead mg/L < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 SAMPLE < 0.005
EP-TOX Mercury mg/L < 0. 0.005 < 0.0005 < 0.0005 < 0.0005 < 0.0005 < 0.0005 ------< 0.0005
EP-TOX Selenium mg/L < 0.005 < 0.005 < 0.005 < 0.005 .< 0.005 < 0.005 ------< 0.005
EP-TOX Si 1 ver mg/L < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 SUBMITTED < 0.05 .,
• . • (!:>
Industrial & Environmental AAalysts, Int'
P.O. 13ox 12846•Reseorch Triangle Porl~. NC 27709•919-467-9919
Date: September 15, 1988
Roge;· Coats
Channel Mester
P.O. Box 1416
Smithfield, NC 27577
Reference: IEA Report No. 350019
Dear Mr. Coats,
Transmitted herev1ith are the results of anal 'Jses on eiiJhl samples submitted to our
lab,ii-atoriJ on Se.ptember 8, 1988.
Please see the enclosed reports for your results.
Very truly yours,
INDUSTRIAL & ENVIRONMENTAL ANALYSTS, INC. ~ ~~7~~ ~~k Randall .
Senior Chemist
Offices and laboratories located in: Essex Junction, Vermont
P-eseorch Triangle Parl1, North Carolina
• FIELD S,\iTLI::G UrFORl-l".TlOM SHEET
Clli\l:I OF CUSTODY 1t1All
(Hazardous ~tacerials and~hers)
::or~: This iur.n ::,ust be completed prior to processing samples in Laboracoc;·. (::a
:5:a:nples will be processed wichout Job ~lo. ,,nd Billing Insc.ructions.)
T.al,nrntory s~mpl~ ~In.:
(I.ab 11',c Only)
Client or System Name: Channel Master ------'-==='-'-===------------------------
Count;·: ---------------------Johnston
Address: P.'O. Box 1416
Date Collected: (c Cc 1i \(J Time Collected: ,'r: (:lcs ----'-'--'----------'-'--'--'--
S ~ r:,p le Lo·c a t !. on or Des c rip t ion : _..,!i!!'!'~!!!!~!._:!_SQO_:!illc_.!f'_!r:.i:0J_Tn1!_1 __:V~OQ_C\;_0__.£CQ0.1Jnc!t3:a~ml1il!nl.iai:ts:e,cdd_.sia.rr_ge~al_ _____ _
at the Oxford, NC Cleanup Site.
Type ot Sar.1pl~: 0 Water O Wast.?watcr O Sludge D llaza."rdous Waste [xJ Ocher Soi
' If Haeardous: Type Code (if any): _________ oar or EPi\ ID 110.: _______ _
Field Infor.nat ion/Comments (or) Samo le Handlin&_ Precautions: _____________ _
I hereby certify that the above ~11form,ation ir correct,
;I I ;,· .• .
I :'. I ( ;·'· Collect·or s Certification: ( fJ,,·'/, • .. ,.: ,., ,'../,·1 ---"-~===-"---'-~-=-'----,------------------! (Signature)
"Sa;;-,rle Allocation" and "Chain of Possession": (Sien & Date in Ink)
l .
2.
J.
Sa.::iple
/) .• ,_Signature Dute T::-::~ (~:-s.
Sar.iple Collector: /L,u .. /,,u ( r;:1<,~: .. (, '· ·.,,r ;,~· -~~~~;---~~-----------1-----------
Sa.r.,ple Transporter:
!\eceived in -L-ab-: -29--~--l;vY.-. -.-,1-l-.U'.o-,1-1,-..,-.J)_-.-.-. ----C/-"7f -5~/I
Analysis Completed: ( \ -------------~-----'------~------
Sar.,p le
lab Test Rea~ested (List Below): Level I
Method 601/602
Lab Silling Instruction: ----------------------------------
• •
Comments BCIL -BELO'W QUi\NTITATIOI-I LIMIT
Purgeoble Holocorbons
I EA Sample No. 350019
Sample Identification At-ea I -Side Slope
Date Analyzed September· 12, 1 9:38
N1Jmber
2
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
'>C" .::... ·-'
26
27
Chlor·omethane
Bn:rmornethane
Vi n1Jl Chloride
Cornoound
Di ch 1 o rod1 f1 uo ro rnBt h3 ne
Ch1on:i.~tfrjfie
r·.-1eth1;lent~ chloride
Tri ct, lorofl uo rn met ha r,e
1 . 1 -DichlOl"oeth;ne
I, I -[)ichlor·oetr,ane
tr-am;-1,2-Dichloroethene
Chloroform
1 _,2-Dic:hlot·oeth;:ini:.
1, I, i -Tr"ichloroett,ane
C.,rbon tetn,::t,lor·ide
8 ro m,idi ch loro methane
1 , 2-Di cJrl o ro p r-o p;rne
tr·er,,;-1,3-[1ichlo1·opropene
Tr"ichlor·oethene
cb-1,3-Dichloropropene
I, 1,2-Trichloroethane
Ch l oro,Ji t, r·orno met t,.1 ne
2-Chlon:,eth,Jlvi n~l ether·
Br-ornoform
Tet r·ac t,1 o r·oet he ne
1, 1 _,2.,2-Tetnichlort)ethane
Cl1lor·otrenzene
1 .,3-Dichlorobenzene
1 ,2-Dichlorobenzene
1 .4-Dicr1iorot,enzene
By Beileq
Ouen~i~etii:1n Limit.
u.q/1'.q
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
i.O
1.0
1.0
1.0
1.0
1.0
1 C1 ' . ,_,
1.0
ID
1.0
1.0
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0 .
!
I
;
Resulfa
Concentration
ug/K,J
· BQL
BQL
BOL
BQL
E,QL
~;(!L
5CIL
E;OL •
BIJL
BOL
BOL
BQL
1
BOL
BQL
BQL
BQL
BQL
BQL
BQL
BOL
BOL
BOL
BQL
BQL
BQL
1E;QL
BQL
E{ll l
•
Comrnent:l BQL -BEL0'•:\1.i~UAI-ITITATION LIMIT
;: .
Purgeob 1 e Aro mot i cs
!Ei\ Sample Ho. 350019 l
Sample ldentificetlor. 1-\t·e;:l 1-Side Slooi?.
By 8;;ile•J
' i!'
Results
l·lumbet· Con1Dound Oui:int.it.1J~iori limit Concentntiog
l\ll/!'.q uq/f~!J
,·, ,.,.~ .
·: .1.,,,.: .. Benzene 1.0 EiCIL ,, Ch l orotienzene 1.0 Bt)L ,_
\ I ,2-Di ch l orobenzene 1.0 BCIL
4 1,3-C,i ch l orobenzene 1 ·1 .l .. BCtL
5 1 4-nirh1 nrnbP17PrtR 1 ,_.1_.111_. _ ~-! ..__. --1.0 BCIL
6 EU· I'] t, -'F -,. ,-1::1 ,e, .:...eiic. 1.0 BCtL
7 Toluene 1.0 B[tl
8 ~:ql ene,3 1.0 EiCIL
• FIELD SAHPLI):G IcfFOIU-LI\TION SHEET
C!IAPI Oi' CUSTODY RECA
(Hazardous ~laterials and ~ers)
1:or~: This t<Jrm :,,use be completed prior to processing samples in Laooratac;•. (::o
5amples will be processed without Job No. and Billing lnstruccions.)
l
Job '.lo. : __ .c.P-"'-'-0"-, _Ne-o~. _4~0~1~5~6~-----Laboratory Sample No.~=-----------
(Lab Use Only)
Clic!:nt or System Name: Channel Master· . ---"'===-==="------------------------
County: --------------------Johnston
Address: P,'0, Box 1416
Date Coliected: 0? S:-cf-7 /<?S15 / . Time Collected:_~/'--"/_(_C_·, ______ ---'-'(~"-~'-s"-'-'.;
Sample ~ocation or Description:_~!'!"""!!!!!!~~s~o~iJlc.Jf2r~o~m~V~O~C;__i:cio~nUt~a~m~i~n~aUt~e~cLl~aur~e~a,_ _____ _
at t~e Oxford, NC Cleanup Site.
Type o'i Sar:1ple: 0 Water O Wastewater O Sludge O llaz,1rdous Waste [xJ Other Soil
If Hazardous: Type Code (if any): ---------oar or EPA ID No.: -------
Field Inrormation/Comments (or) Samo le Handling Precautions: _____________ _
I hereby ~ercify t~at the above info~tia
0
n i~_ .. c:~.re.cc,
Collector s Certification: , . .,C.•-/41/ r ({ i'1..J-,<
1 (Signature)
"Sa;;:i'le Allocation" and "Chain of Possession": (Sign & Date in Ink)
l. l A;' Signature Date
-✓ ---(/ . ( (. ·r
Sar.iple Collector: l..l.•L.· /:'1.:>'" · . .>c",·,\,· ,;.;,·('•. ___ ...,__....:,._,,_ ___ _;,;. ___________ +-'-'-"-"c,..__--+---'-------
tab Test Reouested (List Below): Level I
Method 601/602
Lab Silling Instruction: ---------------------------------
i:·; ~ . ;,;)--~ .
i~~{ ~:i.t~-lr~ · t.;,,t·•'-i•\~ ... it1 • i~lft:::::,.
~.;:;:·~ ·,~mt.ti r~· : : . I':'•'>~ .;r,~:.-..:~-,-~,·· .
:"~,.·t l'lt,ifi' ,··-.-.
!t'-
~!t':f~¥t' C: _ 1i'JJ~li\i.i~.;t71, ... ·,. ~ ,_ :ifJ.t~r Ay, r ~-"~1i'" · ' ~-· 11&:,:
:-: ... -,\J:,J·-.;,
t.'• ~";:•', 1 j {f :iilk~(: ·;:
~;;/!j;,} ..
,., •,,.;1,i;cc····" .. ~;·,\t' -,,~/· :::--;;t~.,}t-:~t;¼r,: ;,: .
f,iJ ir. ,"t'.F;,lif:·-+,: ,;~ -~-1-,.,
•;c,f }t~;t-;•,'
/:! ft.~?~~~---.
.f:.\ •· ~t .-
.;.~'; , ..
,.---"I'!',,-.
.L. iK~~-: . -· .....
• •
Comments BC!L -BELOVi OUMITiTATION LIMIT
Pur~eoble Holocorbons
IE/\ Sample Ho. 350019
Sample Identification Area,! -Adjacent t•J Fence
Date final yzed September 1 2, 1988 By Bai1eq
Number Cornoound
Chloromett,ane
" Brnmometh,ine ~
7 ,, 'ii nyl Chloride
4 Diehl o nn1i 1l 1Jo 1-0 met h,J ne
" ·-' ChloroetMne
6 MethtJ1ene chloride
7 Tri ch l or oil uo ni meth;J ne
r, 0 1, 1-Dichloroethene
9 I, 1-Dichlor·,:,ethane
10 tran:::-1,2-Dichloroethene.
11 Chloroform
1 '' '-1 )2-Dichlor-,:n:!th::!ne
13 1, l, 1 -Tr-ichloroetr1ane
14 Carbon tetrechloride
15 Bro modi ch lo 1-ornet ha ne
16 1,2-Dichlorop1·opane
17 tt·eno-1,3-Dic,hlor·,:,pt·opene
1 ,, ,_, T richl o roet he ne
19 ch-1,3-C•ichloropropene
20 1, 1 _,2-TrichloroettvrnB
21 Chlorodi bromometh8ne
?? 2-Chl,iroeth,Jlvi nyl ether --23 Brornofor·rn
24 Tet r,1chl oroet he ne
·'") C" L,' 1, 1 .,2,2-TetrechJ,:,n:,e'thane
26 Cl1lor·otrenzene ,, ., 1,3-Dichloroben:ene ~'
'"•O L ,_, 1 )-Dic:hlorobenzBne
29 1 .4-Dichlor!Jt,enzene
Results
Ou8nf.itati,Jn Limit C~• r!•::e nt ration
U•J/Ko u~/Kg
.0 BQL
.0 E:OL
.0 BQL
.d BQL
.0 BOL
1.0 BQL
1 0 Bi.IL
1.0 B!JL
.0 BQL'
.Cl BQL
0 BQL
.0 BQL
.0 BOL
[i BQL
I.Cl BQL
10 E:QL.
1.0 8QL
1.0 E:IJL
1.0 BQL
1.0 BQL
1.0 BQL
1.0 BQL
1.0 BQL
t .0 Bi.IL
i .0 . BQL !~
1.0 BQL
1.0 BQL
1.0 BQL
1 , 1:1 BQL
,:-". . . ~ ..
-~~\·'· .. ;\ _'.
lt~1~/ /~1,,·~-... ,, ...
i'.:tj,z~ ,·.
i~~~-•-1'~¥-t ~' m11i1&•:. ,: · · ~11tF;t-·· ~~-;~J~!,~{/ . ;.f~1,f.5<t,'i:-~--· .. ill;,,_·.
\;~r:tt:-•: . ·
! ',_._, •)• ···1 :i;: ·'
":.\'.,: -~· '·' ~-~ ·, .. ,..-<--. ,.,,,,.
• •
Comments BQL -BELO'W OUAMTITATION Li MIT
Purgeabl e Aroma ti cs
IEI\ Semple !!o. 35001 '"
Sample Identification Area 1-Adjec:enl to fence
Dete l\nal ~zed· '.3eotember 12 1982:
!•lumber·
4
C: ·-'
6
7
8
Compound
Benzene
Ch l orot,enzene
'1,2-Di cb l ornt,enzene
.1 ,3-Di ch l ornt,enzene
1,4-Di ch l ornbenzene
EtJ11:11 benzene
· Toluene
8~ Cur-rq
Ouantitation Limit
' .
ua/K1J
0
0
.0
0
.0
1.0
1.0
1.0
,j
l Results
Concentr·ation
uq/Kq ,,
BQL
BQL
BQL
Bl)L
BOL
BOL
2
BQL
• FIELD SAIPLI::G U!FORMATION SHEET
· CIIAI:1 Of' CUSTODY RECfA
(Hazardous ~aterials and O~rs)
::or::: This fvr.n :nust be completed prior to processing samples in Labor.1to:-J, c:o
sa~ples will be processed without Job ~lo. nr,d Dilling Inscruccions.·)
Joi:, :10.: r. o. Nn. t,0156 ---'-'-=---'-=-=-=c.....------Labor;icory Sample '.lo.: ------------(Lab Use Only)
Client or System Name: Channel Master ----'-==--=~===------------------------
Countj·: ---------------------Johnston
Address: P.'O. Box 1416 -----'--'---"-'----'=-'--'-'--"-"---------------------~------------
Time Collected: I I ,·,c__: ;(~cs.) --~~---------~--~
S~nple Location or Description: _ _!~"'!!"'!!!!!~~s~o2i1lc.Jfjr~o~m~V~OQIC~cQO~n~t~a~m~i~n~;i~tte~c11_!!aLr~e~a!._ ______ _
at the Oxford, NC Cleanup Site.
Type of Sar:ipli?: D Water O W,i)st~water O Slucl£c O Haza."rdous Waste [D Ocher Soil
If Ha:ardous: Type Code (if any): ---------oar or EPA ID tlo.: ---------
Field Information/Comments (or) Samo le Handling Precautions: _____________ _
. I hereby certify that the above inf?nnation i~ cprrect, /) I .. /
Collector's Certification: t!.c,. -·· .. ,• f (,<,,__,,, -----'--===-+------'---,-.------------------(Signature)
"Sa:::;,le Allocation" and "Chnin of Possession": (SiGn & Date in Ink)
Date. (1~,/,, 3igna~.ure
. ,/'
I. Sanp le Collector: ( le'; . ../ { ~
,
(.--• i r ·1 .'
2. Sar.iple Transporter:
J. Sar::ple Received in Lab:
k. Sa.;:iple Analysis Completed:
Lab Test Reou~sted (List Belau): Level I
Method 601/602
Lah 5illi~5 Instruction: -----------------------------------
Special Ins,ructions or Comments1_~3~-~D~n'-'-_T~u~r~n~a~r~o~t~,n~d"--~'_'\~i~'-'~·-·~//-'--"-"~;·~,_·/~~-(~;;,~·,+1'--\~,~~·~(~,. __
</el<:_
' »·
. : ; '"~:--·.
··:. '""'.':.';-'•" !.£., :;•'.:\ .. ;-: ,; ~-··~t _:,;.
, ,.~;,1,. .•. ·
. -, .l• /. ~-'.~•-·_;_
i;:.· --~-, .
s'•" i;\i\''.
:;·.: .. ..:.· ,., . . . .,.,.t _•,
._ ;I> ·•·'• ~.:. ,_:: .-. :... . ,:.._ .... ti",_ .
_::':· t?~~.': -
• •
Comments BQL -BELOW QUAIHITATION LIMIT
Purgeoble Holocorbons
I El\ Sample No. 350019
Sample Identification Area I-Build. Side :3looe
Dote /\nalyzed September 12. 1988 lly Corn·-,1ell
Number
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
'ir, ... o
29
Compound
Chloromethane
Bromomethane
Vinyl Chloride
Diehl o rodifl uoromet ha ne
Chlo roet 11a ne
Meth1Jlene chlot·ide
Trichlorofl uoromethane
1 _, 1-Didiloroethene
1, 1-Dichloroethane
trans-1,2-Dichlc,1·oethene
Chloroform
1,2-Dictiloroethane
1, 1, 1-T1•ichio1·oeH1ane
Cirbon tet1·achloride
8 ro modi ch lo ro methane
I ,2-Dich101·,:,propane
trans-i }3-Dichioropropene.
T richloroetf1ene
cis-1,3-[iichloropropene
1, 1,2-Trichloroethane
Chlorodi bromomeH1ane
2-Chloroe\htJlvin1,l ether
Bromoform
Tet r,ict,1 o roet hene
1, 1,2,2-Tetrachloroethane
Chlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
1 .4-Dichlorobenzene
I.
Results
Ouanti\a\ion Li mi\ Co nee ntratio n
ug/Kq ug/Kg
1.0 · E:QL
1.0 BQL
1.0 BQL
1.0 BQL
1.0 BQL
1.0 BQL
1.0 BQL
1.0 BQL· ,.
1.0 SOL
1.0 BQL
1.0 BQL
1.0 BQL
1.0 BQL
1.0 E:QL
1.0 BQL
1.0 BOL ·
1.0 BQL
1.0 BQL
1.0 BQL
1.0 BQL
1.0 BQL
1.0 SOL
1.0 BOL
1.0 BQL
1.0 BQL
1.0 BQL \
1.0 80L
1.0 BQL.
1.0 .I BQL
• •
Comments BQL -BELOW QUANTITATION LI MIT
Purgeob 1 e Aromot i cs
IE!\ Sample No. 350019 l
Sample Identification Area 1-Build. Side Slooe
Date Anal 112ed September 12, 1988 By Currq
Results
Number· Compound Ouentitation Limit Conc.,ntretioQ ·
uqiKq uq/Kq
Benzene 1.0
.-, CJ1 l orobenzene 1.0 BQL I ,._
' 1 ,2-Di ct·1 l ornt,enzene 1.0 BQL
4 1,3-Di c:11 l ornt,enzene 1.0 BOL
cc 1 ,4-Di clil orobenzene 1.0 BQL _,
6 Et111~lbenzene 1.0 BQL t.
7 Toluene 1.0 11 '
8 ;~yl enes 1.0 2
• FIELD S"'"l'LI>:G DfFOR!-t<\TION SHEET
CHAI:! Or CUSTODY RECcA
(Hazardous Materials and ~rs)
~:or;:: This form ~ust be completed prior to processing samples in Labor3tory. (~:o
sa~ples will be processed without Job }lo. ~nd Dilling Instructions.)
Laboratory Sample No.: Job '.lo . : __ ,.:P:..;•c._;O::c';..,..:N.:.,o'-'.'-4'-'0'-'1'-'5'-'6"--_____ _ ---------.,.---(Lab Use Only)
Client or System Name: Channel Master ---"==='--'===-------------------------
Count;-: Johnston ----------------·----
Address: P.'O. Box 1416
Dace Collecced: ~ Sc;? 19 S'S Time Collected: (/ :-[) (:-l:s. l -~~~~-----------
Sanple Location or Description:_~~~~~~~s~o~iJlc..Jf~r~o~m!!_V~O~C__.s:c~o~n~tJa~m~i~n~as!..!;_tgegd_,lair~e~aL_ ______ _
at the Oxford, NC Cleanup Site.
type of Sar.lplt?: 0 Water O t.J'ast.?water O Sl.udcc O llaz.a."rdous Waste (KJ Ocher Soil
If Haeardous: Type Code (if any): ---------DOT or EPA ID tlo.: ---------
Field Iniormation/Comments (or) Samo le Handling Precautions: ______________ _
I hereby certify that tl,e above information is correct,
,/; f' ,' ,/· '
Collector's Certification: ,_.:'(J/l:: ';-/.,.:·c ·., _.,,L::,-="-'-+'----"-=--;->----'--'---c---------------
l (Signature)
"Sa;,,ple Allocation" and "Chain of Possession": (Sign & Date in Ink)
,, ,
// /' ,, '
I. Saraple Collecto,: /-~~/_I •·•;•
Signat:ure Date:
2' Sample Transpot'te,:
J' Sar:iple Received in Lab:
(_
~' S.;.::ip le Analysis Completed:
Lab Test Reouested (List Below): Level I
Method 601/602
Lab 31lli~, Inst,uction: -----~-----------------------------
' ...... '
-~· . ~•' ·.; .... <· ..... r,!:. . .')' f,_ .
< "\' .:~:-,
•••. · .. :· ! • ~
.. ,;.;.,
... ,-
•• •
Comments BOL -BELOW QUANTITATION LIMIT
Tetrachlor·oethylene and 1 _, 1,2,2-Tett-achloroethane coelute. GC/MS
M1al1Jsi:l is recommended for· confirmation.
Purgeoble Holocorbons
IE!\ Sample !fo. 350019 _±
Sample Identification l\t"ea I-Bottom
Date !\nal yzed :3eotember· 12 1988
Number Compound
Chloromethane ,, Bro mometha ne '-
3 Vi n1Jl Chloride
4 Dichlorodi!l uot-ornethane
5 n, 1 oroet h,ine
6 Methylene chloride
7 T richlorntl uoromethane
6 I, 1-Dichloroethene
9 1, 1-Dichloi-oetha~~
10 trans-I,2-Dichloroethene
11 Chloroform
12 1,2-Dichloroethane
13 1, 1, 1-Trichlor·oethane
1 4 Carbon tetrachloride
15 B rnmodi chi o i-ometh,i ne
16 I,2-Din,Joroprop;;ne
17 trans-1,3-Dichloropropene
18 Tri c r,1 o roett,e ne
19 ci3-1,3-Dichloropropene
20 1 , 1 , 2-Tri c h1 o r·oetJ,,rne
21 ChlorOiJi bromomettm,e
~? 2-Chlor,ieth,J1Vi rt1Jl ether ......
}7 ~--Bromoform
24 Tet rac ti l oroet lie ne
?CC ~-· 1, 1,2,2-Tetr·achlsiroethiine
26 Chlorobenzene
27 1 ,3-Dichlorobenzene
28 1 )2-D;chlot·obenzene
29 I .4· Dichlornt,enzane
By Corn·-.-.-·ell
Ouantitation Limit
gq/Kq
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Results
Co nee nt ration
~
BQL
BQL
BQL
BQL '
BQL
BQL
BQL
f;QL '·
BOL
3
BQL
BQL ;
BQL
BQL
BOL
E'OL
BQL
46
BQL
BOL
BOL
BQL
BQL
19
BQL
BQL
BQL
BQL
80L
•i:·
.:• · .. • ,1~-.
• •
Comments BQL -BELOW QUAt-lTITATION LI MIT
Purge!lble Arom!ltics
IEA Sample No. 350019 .:!
Sample Identification Area 1-Bottom
Date Analyzed :3eptember 12, 1988
Number Com Mund
1 Benzene
2 Ch l orot,enzene
3 1 ,2-Di cr1l orobenzene
4 1,3-Di c:111 orobenzene
5 1,4-Di chl orobenzene
6 Ethyl benzene
7 Toluene '
B Xyl enes
By Corn\•lell
Ouantitation Limit
gg/f'.q
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Results
Con(:~ ntrati on ..
u.q/Ka
BQL
BQL
BCIL
BQL
B!JL
BQL
6
BQL
•
FIELD S"-"''.l'LI'.:G UfFOR!-IATION SHEET
C!IA 1:1 Or CUSTODY REC.
(Hazardous '.1aterials and O~rs)
;:or::: This f.:,rm ::iust be completed prior to processing samples in LaborJtuCi'• (::o
sa::iples will be processed without Job Ho. nnd Dilling Instructions.)
Joi, './ o . : __ .,:P_;•e,_:O::.:•c......,N.:,o::.:·c......:4:..:0""1"'5'-'6'-------Labor~tory Snmplc ~lo.~: __________ _
(Lnb Use Only)
Cl!.c:nt or System Name: Chnnncl Master -------~~~----------------------
Count;·: --------------------Johnston
Addrass: P.·o. Box 1416
/ (' Dace Collected: ~· .• ~-r S( Time Collected: (il~s. l --------------~
· San p l _e Lo ca t i on o r Des c ri p t i on : -~!!~~~~s~o'.2:i:J. l~f1r:_c:0~11!._1 ~V~O~Cc..' 1c~oc1_nl_!t;_,· a!i:rni1_1il_!1!.!1 al_!t;.!e~cLI _;_a)Jr[!e2;i3_ ______ _
at the Oxford, NC Cleanup Site.
Type oC Sar.iplt?: 0 Water O Wast.:?wnter · 0 S1.udric D 11.Jz.~lrdous W,,stc (KJ Ocher Soil
If Ha:adous: Type Code (if any): ---------Derr or EPA ID tlo.: ---------
Field Information/Comments (or) Sarnole Handling Precautions: _____________ _
I hereby certify· that the above inforrriativn is correct,
·) /' .
C l , I • • /, ,(··, . , o _actors Certtflcation: /i re .',, '1.·. ,, ,, _ __ .,_-'-'--'-'-'-------~---,----------------~-/ (Signature)
"Sa:.:ple Allocation" and "Chain of Possession":
Sir.nature
. .
I. Sar.iple Collector: .'( · .. ( ( ,,{·. (. , ..
2. ?=ple Transporter:
3. Sar.:p le Received in Lab:
~. Sc:L~p 1 e Analysis Completed:
Lab Test Reauested (List Below): Level I
Method 601/602
Lab Silli~, Instruction:
(Sign & Date in Ink)
Date
((
I Z: uc)
---------------------------------
Spec!a 1 Ins,ruct ions or Comments: 3-Dny Turnnrouncl / L·,. I /I.·, 1, 1., ./, ;·.:· ,/-ti .!.( c, ~ ill l, !) l(;; _____ .....,_ ____ ......,_--'-'-~~__,--------,--------
• •
i • '':
. ': .. .,
Comment1 BOL -BELOV-/ QUMITITATION LI MIT
·:-,_• '.-.-. Purgeable Halocarlrnns
I El\. Sample No. 35001 9 2
Sample Identification Area 2-Adj. to ditch
Date Anal ~zed September 12. 1988 By Corn-,-,1ell
Results
Num~er Compound Ou;,ntitation Limit Concentration
uq/K•J ll.c/Kq
Chloromethane 1.0 BQL
2 Bi"c1momethane 1.0 BQL ., Vinyl Chloride 1.0 SOL ,'
4 Diehl o rodi fl uoro met. hane 1.0 BQL
5 Chloroe\hane 1.0 SOL
6 Methylene chloride 1.0 BQL
7 T ricMor·on uor-omethane 1.0 BOL
3 1, 1-Dichlornetr,ene 1.0 8QL ,.
9 1, 1-C,ictrloroethane 1.0 BQL
10 trans-1,2-Dichloroethene 1.0 BQL
11 Chloroform 1.0 BOL
12 1,2-Dichloroettm,e 1.0 M 8QL
13 1, 1, 1-TricMoroeth,ine 1.0 BQL
14 Carbon tetrachlot"ide 1.0 BQL
15 B r·o modichl o r·o rnetha ne 1.0 BQL
16 1,2-Dichloropropane 1.0 8QL
17 trans-1,3-Dichloroproper,e 1.0 BOL
18 Tri ch loroet he ne 1.0 1
19 cis-1.,3-Dichloropr-opene 1.0 BOL
20 1, 1,2-Trichloroethane 1.0 BQL
21 Chlorodi bromomethane 1.0 BQL
22 2-Chloroethr;lvi nyl ether 10 BOL
23 Bromoform 1.0 BOL
24 T et rachloroet t,ene 1.0 E;QL
25 1, 1,2,2-Tetraa::hloroeth;,r,e 1.0 BOL
'f 26 Chlorobenzene 1.0 BIJL
27 1,3-Dichlorobenzene i.O BQL
.: 28 1,2-Dic:hlorobenzene 1.0 E:QL
29 I .4-Dichlor·otrenzene 10 BOL
!
~r •:., ·-i~r:t{~ : ...... _,.
' ,.
} :~·~:1r:· · ·
·, ,:: :.1~\-
••• '•! ••
,. • ~<~ .. • A. 0
. ·. ,.'/'\ . . .,, '
rr~ ::.: ·-\•i
.. -.:,,;..;>.
,; '",' -;~!.'.'
.·•.,) .... ,,.,
. ' . : t-:, -, ••• ,..., t . '~.
.. _.· .];~!;.-~' :;::/f;/·
·,1::-_tl:
• •
Comment3 BQL -BELOW QUANTITATIOM LI MIT
Purgeoble Aromatics
I EA Sample Ho. 350019 2
Sample Identification Area 2-Adi. to ditch
Date Analyzed September 12. 1988 · By C•irnvell
Results
Number Compound Ouantita\ion Limit Co nee nt n,tl on
u.g/Kq ug/l~q
Benzene 1.0 B[ll
2 c1·1 l orobenzene , r1 I.' ... BtJL
3 1,2-Di ch l orobenzene 1.0 BOL
4 1,3-Di ch 1 orobenzene 1.0 BQL
5 1,4-Di ch 1 orot,enzene 1.0 BOL
6 E t111dl benzene 1.0 BCIL
7 Toluene 1.0 C ·-'
8 '(lj' p•·•p<· I ._ t _-11 _ .. :, 1.0 BCIL
FIELD S,\..'!PLI):G I}!FOR1'1ATION SHEET
· , CHAnl OF CUSTODY REcA
(Hazardous '.1at~rials and -'11'!',ers)
~:or::: This f,,rm '.'1'JSt ':,c completed pri :,r co proccs!.inc samples in LaOor~n:o:-;·. (~:o
5~~p~es will be ?recessed without Job No. arid Billing Instructions,)
J O b : 10 • : ----'P--'.-'o'-.'-'-N--'nCC.C--/'-'1 0'-1'-'S'-(i'-, ----Laboratory Sample No.~: __________ _
(Lab Use Only)
Client or System Name: Channel Master '-'----"'===--'-"=='-----------------------
County: Jol1nston ------'-'-----------
Address: P.'O. Box 1416
Dace Collected: lo Se) { <( \:?( Time Collected:_:./_/_;_n_··c_) _______ (~~~~~s..:...
Sanple Location or Description:_~~~~~~s~o~-:~1~.Jfj·r~o~m!!....!V~O~C;;_ic~o~1~1t~,~11~ni~1~1a~t~e~dLa~rLe~ai!_ _____ _
at the Oxford, NC Cleanup Site.
Type of Sar.iple: 0 Water O Waste .... ·ater D S1.udcc O llaz.~lrdous Waste (KJ Ocher Soi]
If Ha:adous: Type Cede (if any): DOT or EPA ID 110.: --------
Field Inf orna c ion/Comments (or) Sample Hand ling_ Precautions: __ .....,.. __________ _
I hereby certify that the above information is correct, f, /) )'
Co 1 ! ec c or's Ce rt if ica t ion :_-+'/'..c:-'c::<-:.c·"::..···:.../:...,'/__~,t-''/ _ _:'i:-,_· -~I'--"-;:_· ·c,r :..:'::.../.c.'o.-'----::-----------------
7 (Signature)
"Sa:cple Allocation" and "Chain of Possession": (Sign & Date in Ink)
I.
2.
J.
Sar.iple
Sar.iplz
S~r.ip le
S2..,ple
Collector: 1c20L /-1
:/.-~~-:~--~ I~-~;~~(,! ~~~;. ,CH:s.) ~'--"";_:_'---'-''½1''---~""-'---"'-"-"--''--------t-'--'-''---"-'-'-+--'--'-"-'----
T rans port c r:
!\ecP.ived in -La_b_:_~----"..t=:=-_,,~=(,::..:~~(!_~Cc:Q°'-"""'-''~..::.:l,\)=,__ ___ -l-c-'-1-'-:J""·-··-~1..::_.-+-"--/;J._:_u_:o __
Analysis Completed=-----------------'------'-------
lab Test Reou~sted (List Belov): Level I
Method 601/602
lab Silli~, Instruction: ----------------------------------
v u ,
--· . ' t. '7.. . \ .
·;• .. /, 'l ·.:• •..
f· ' .. ...... ' ', ".''
1,: ,. ,.
;, t • •
Comments BOL -BELOW QUANTITATION LIMIT
Purgeob!e Holocorbons
I EA Sample Ho. 350019 6
Sample Identification Area 2-Adj. to Drqer
Date Analyzed September 12 1988 By Currq
Number Compound
1 Chloromethane
2 Bromomethane
7 Vi n1J1 Chloride c•
4 Di ch 1 o 1·odi fl uo ro methane
5 Chloroethane
6 Meth,Jlene chlor·ide
7 frichlorn!l uoromethane
r, C, 1, 1-C1ichlornethene
9 1, 1-Dichloroetha'ne
10 tr·ans-1,2-Dichlor-oethene
11 Chloroform
12 1,2-Dichloroethane
13 1, 1, 1-frichloroetr,,ine
14 Carbon tetrachloride
15 B r-omodic hl o ro methane
16 1,2-DicMoropropane
17 trans-1,3-Dichloropropene
18 Tri c hlo 1·oe\he ne
19 cb-1 ,3-Dichloropropene
20 1, 1.,2-Trichloroeth,ine
21 Chlorodi bromometr,ane
22 2-Criloroethylvin,Jl ether
23 Brornoform
24 Tetracril oroet he ne
,, C, 1, 1,2,.2-Tetrtlchloroethane ~-· 26 Chlorobenzene
27 1,3-Dichlorot>enzene ,,~ c:..O 1 ,2-Dir; hlor1:i benzene
29 1 ,4-Dict,loroben,ene
Results
Ouantitatior, Limit Concentration
uq/Kg ug/Kg
1.0 BQL
1.0 BQL
1.0 BOL
1.0 BOL
1.0 BOL
1.0 BQL
1.0 BCil
1.0 8QL ,,
1.0 BQL
1.0 BQL
1.0 BQL
1.0 8QL
1.0 BQL
1.0 SQL
1.0 BCIL
1.0 8QL
1.0 BQL
1.0 BQL
1:0 BQL
1.0 SOL
1.0 , BOL
1.0 BQL
1.0 BQL
1.0 E;QL
1.0 BQL
1.0 81JL
1.0 BQL
1.0 E:QL
1.0 EiQL
•, ' . ,. .-~· -::i :;.~,,: : ... • • ~ .. ·"" ::~?<C(;· :· :
Commen\3 · BQL -BELDW QUANTITATIOt·I LI Mil
Purgeobl e Aromot ics
IE/\ Sample No. 350019
Sample Identification Area 2-Adi to Drqer·
Date t.nal11zed Seotember 12 19:38 By Currq
Results
Number Compound Quantitation Limit Co nee nt ration,_
u.g/!'.g LUJ/Kg
Benzene 1.0 Bl)L
2 D1lorobenzene 1.0 BQL
3 1 ,2-Di cl11 orobenzene 1.0 BQL
4 1,3-Di cl11 orobenzene 1.0 BQL
5 1,4-Di ch 1 orobenzene 1.0 BOL
6 Ell1~lbenzene 1.0 BOL
7 Toluene 1.0 ,-,
L
B X1Jl enes 1.0 BQL
A FIELD S"'~LI'.:G U!FOR!-tl\TION .-.LEET
~ · Cl~IN OF CUSTODY RECO.
(Hazardous ~aterials and Others)
~.'OT~: This (orm ::iust be completed prior to proccsr.inc sampl~s in Labor.:itor·;. (~:o
sa~ples will be processed without Job No . .n11d llilling Instruccions.)·
Job :10.: r. o. No. t,01.56 ------'--'~-~=------Laboratory Sample No.~: __________ _
(Lab Use Only)
Client or System Name: Channel Master --~~==~===--------------------------
County: --------------------Johnston
Address: r.·o. Box 1416
Date Collected: 07 )(f' /ff..f Time Collected:_~/~/_{!_C_J _____ --'(-~-~~s_.-'-)
Sanple Location or Description:_~~~'!"'!!'!~s~o~ill;__!fjrlo~mGV~O~C0c~o~nut~a~m~iun~aut~e~dLJa~rue~aL ______ _
at the Oxford, NC Cleanup Site.
Type o[ Sar:iplt!: 0 Watet· 0 t.Jnsc~wa.tcr O Sl.udcc O 11.nza.rdous W.,stc EJ Och~r Soil
If Haeardous: Type Code (if any): ---------DOT or EPA ID tic.: ---------
Field Information/Comments (or) Samole Handling Precautions: --------------
I hereby certify that the above information if correct, iJ // //
Collector's Certification: ___ ~};'--"-_~./.~.1.~,/_';+'t_~·f_f~'._·c_·,_,.~"-•-· ___________________ _
( (Signature)
"Sa:::ple Allocation" and "Chain of Possession":
/
(Sign & Date in Ink)
~. Sa.::iple Analysis Completed: -----------------~------------
Lab Test Reouested (List Belo~): Level I
Method 601/602
Lab 31lli~, Instruction: ---------------------------------
• •
Commenti BQL -BELOW QUANTITATION LI MIT
Tetrachloi-oethylene ,;nd 1, 1,2,2-Tetrechloroethane coelute. GC/M:3
anal 1Jsis ls re(:ommended fot· confi rrnation.
PurgeHble HHlOCHrbons
I EA Sample No. 350019 l
Sample Identification Ai-ee 2-Adj. to build.
Dato Anoly20d ~;eptember 13. 1988
Number
2
4
5
6
7
9
10
11
12
13
14
15
16
17
18
19
20
21
·22
23
24
25
26
27
28
29
Chloromethane
Bromomethane
\'i nyl Chloride
Sompound
Diehl o rodi fl uorornet hene
Chloroett,ane
Me\h1Jler1e chloride
Trichlorofl uoromethane
I , I -Dichloroethene
1, 1 • Dichloroelhane
tr·ar,;.-1,2-Dicr,loroeH,ene
Chloroform
I _,2-Dichlot·oethane
1, 1, 1-Trichloroethane
Carbon letrachlot·ide
Bromodichlornmethane.
I ,2-Dichloropropane
trans-1,3-[)ichloropropene
Tt·ichloroethene
cis-1,3-Dichloropropene
1, 1,2-Trichloroethane
Chloro,Ji bromometh:ine
2-Chloroe\h!Jl\li fllJl ether
Bromoform
Tetrachloroethene
1, 1,2,2-Tetrechloroe\hene
Chlorobenzerie
I ,3-Dichlorobenzene
1,2-Dichlorobenzene
1 .4-Dichlorobenzene
By Bailey
Ouentitation Li mi\
i1.q/Kg
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
1.0
1.0
I .D
1.0
1.0
1.0
1.0
i.O
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Results
ll.q/Kq
·BQL
BOL
BOL
BQL
BOL
BQL
SOL
BOL •
E:QL
BQL
BQL
BQL
BQL
BOL
BQL
B1~L
BOL
E,QL
BQL
BQL
50L
BQL
BQL
7
BQL
BQL
BQL
BQL
BQL
,' .. ,· .. .,_ . : .. .-,;,:, • •
Comments BQL -BELOW QUANTlTATION LI MIT
Purgeoble Aromatics
I EA Sample No. 350019 l
Sample Identification Area 2-Adj. to build.
Date Analyzed September 13, 1988 By Boileq
Results
·-•. J. •.• ,., •• . 1. Number Compound Ouantitation Li mi\ Co nee nt 1·,;tio n,
ll.Q/}'.g wi/r:g
Benzene 1.0 BQL
2 Ch 1 orobenzene 1.0 BQL \ 3 1,2-Di cl1l orobenzene 1.0 BCILi
4 1,3-Di ch 1 orobenzene 1.0 Bl)L
5 1.4-Dichlorobenzene 1.0 BQL
6 EU11Jlbenzene 1.0 B(JL
7 Toluene 1.0 2
B 11w1 ono•' n.. ,.. , .. .:, 1.0 E,QL
• FIELD S,\.'fPLI::G UIFOR!·IATI-. SHEET
CllJ\1:1 OF CUSTOD'( I\.D
(llnzardous '.!ntcri.1 Ls ;incl Others)
~:or::.: This fur.n ~ust be comrlctcd prior to procc5~inr, s,,mpl~s in L1Dor.:1to:-i'• (~:o
5a:nples will be processed without Job ~lo. ;ind Billing Insc.ructions.)
Jo b '.Io • : __ _c.P...c·---.:Occ.__...c.Nc..coc.c,'-4~0c.clc..a5cc6~------Labor;itory S;imple No.: -----------(Lab Use Only)
Client or System Name: Channel Master ----===='-'-===------------------------
Count;·: ---------------------Johnston
Address: r. · O. llox Jlil6 -------'--'-~--.,.-------------------------------
Ti rn e Collected:~~-'·•_;_J _________ (~~-"~s
Sar:iple Location
at the Oxford, NC Cleanup Site.
Type oi. Sar.1ple: D \.later O Wast.?watcr O Sludge O Hazardous Waste (KJ Ocher Soi
If Haeardous: Type Code (if any): DOT or EPA ID tic.: -----------------
Field Information/Comments (or) Sarnole Handling_ Precautions: --------------
I hHeby certify chat the abov~,/nf~rrnation/~ correct,
Co 11 e c tor ' s Ce r c i f i ca t ion : __ "/2~' :~>~c~-,..f~> -'"t..f'--'~i·_· ~;_'._· ·.,..· _'· ._'_,~\---.,--------------------
/ (Sic11;it11rc)
"Sa..:ple Allocation" and "Chnin of Possession": (Sign & Date in Ink)
I.
2.
J.
,') ;,) Si~naturc
SatJple Collector: /C.c.cl:~r.,,, i;· 1;:ll ,.:...Jd {,·• f' 1,s· \·_·) --~~-/-~~~~~--------1~----+-~-~--
Sar.ip le Transporter: -----~---iol--------------1--,.------,+-------
S an pl e !!.eceived in Lab: rf},w, ,tlJlLo'cc-H0L l}-'li -'j( l~ u-0
___,___=:c......,.\u---"....C.-=-=-=--=.;:_'--'='----1~--""'---i--\ -'-=---~
s,_;:iple Analysis Completed: -------------------------------
D~tc
Lab Test Reauested (List Below): Level 1
Method 601/602
Lab 51lli~g Instruction: ----------------------------------
SP e d al Ins -rue t ions or C ommcn ts : _-'3,_--'l_ln.:.y,_·;.;r1 .. 1 r"", 1.,,,rn-'-r"'o'-1""rn"'<"'l ___ ._/_,/ __ ,J_' ,,_:_,_l __ .. ,._'l_::.1_.' _:_(_(_' ,_/_··f_c_: 1_'-_l __ _
' . ..,. ·1•:·:; .-
.';: .. ·:~; '.'
-~ .:.:·.
·.'{,
•• ·-~'< •• '
•·• r ,: • .-. ' .. . . ,,.,•.,., .. -'• •.. , ' ..
~:~.<~},·: ,' ...
• •· •• •V, ·-·:r
,•·. •'., .. ,i ,._ •. .. ~ -..
. -·;' :'.' '. ;: ,''., .· ., ....
• •
Comments BQL -8EL01N QUANTITATION LIMIT
Purgeoble Helocerbons
!EA Sample Ho. 350019 fl
Sample Identification Area 2-Bottom
Date Analyzed Septem~er 13. I 988
2
3
4
6
7
8
(l
10
11
12
13
1 4
15
16
17
1:3
19
20
21
26
27
,-,,:, t.. ,_,
29
ComDound
Chloromethane
8 ro mo met h,i rre
Vi ntJl Chloride
Dict,lorodi t7 uoromethane
Chloroetharre
Me\htJlene chloride
Trichlorofl uoromethane
1, 1 -Dict,loroethene
1, 1-['ichloroe\hane
lrans-1,2-Dicr,loroethene
Chloroform
1,2-Dichlot·oethilne
1, 1, 1-Trichloroethane
Carbon tetrachloride
8 ro modi ch loro methane
1,2-Dichloroprop,rne
trans-1,3-Dichloropropene
Trichlor·oelhene
ci3-1 ,3-Dichloropropene
I, 1,2-Trichloroethar,e
Chlorodi brornometh3ne
2-Chloroeth•,lvi ntJl ether
Bromofor-rn
Tet r·ac h 1 oroet he ne
I, 1,2,2-Te\rachl(,rMthane
Chlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorotienzene
1 .4· Dichlorob~nz,rn~
By Curry
Results
Quantita\ion Li mi\ Concentnition
uq/Kg ,' l-' ~
1.0 BQL
1.0 E:QL
1.0 BQL
I.I) BQL
1.0 BOL
10 BQL
10 BQL
1.0 BQL
1.0 BQL
1.0 E:QL
1.0 BC!L
1.0 BQL
1.0 BQL
1.0 BQL
1.0 BQL
1.0 BOL
1.0 BQL
1.0 9
10 BQL-
10 BQL
10 BQL
1.0 BQL
1.0 BQL
10 EiC!L
10 BQL ·.·
10 BQL
10 BQL
1.0 E:QL
1.0 BQL
,:.) < ~-~·,. '·~ ':.'/' ·.:1:;1 .' _. .·
_:\:· '.;¥£:?· : ~'
,. ·'~~-~< :-
!, ,'
:J.;','., .,;;:,; ..
. , ·,, 'i~~t ..
. ;: . ~r_;,.-... :
,. ff~·'
I --, .,,~ t ••~' ,
• '<.'.~• ..
'.;"", .:'.'{;,~···
'! vl • ·;.:,
'l'J:-
:. ·,· -~-,
•
Comments BQL -BELOW QUANTITATI0N LIMIT
Purge11ble Arom11tics
I Ell Sample No. 350019
Sample Identification Area 2-Bot\om
Date l\nalyzed September 13. 1988
Number
2
3
4
5
6
7
8
Compound
Benzene
Ct-1 l orot,enzene
1 ,2-Di ch l ornt,enzene
1,3-Dichlorobenzene
1,4-Di cl1 l or-obenzene
ElJ1qlbenzene
Toluene
By CutT'J
Ouantitation Limit
nq/Kq
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Results
Con,entr~tiof\ .
ggl_lg_
BQL
BC!L
BIJL
BQL
BCIL
BOL
BOL
· BQL
• •
September 21, 1988
TO: File
FROM: Jack Butler
SUBJECT: Telephone conversation with Roger Coats (919-934-9711)
about Channel Master, NCD122263825
Mr. Coats contacted me on this date at the Ulah Battery site
to request a meeting to discuss a work plan proposal for phase II
of the clean-up at the subject site. This work plan will discuss
monitoring on site to define extent of contamination but not an
extraction well or other clean-up method. Mr. Coats also
reported that he had some analytical data on soil that has been
treated in the on-site rotary dryer. Mr. Coats agreed to send a
copy of this data and the work plan to our office in Raleigh for
our review. Mr. Coats was informed that I would be on the Ulah
Battery site for most of the next 3 weeks, however, I agreed to
review the work plan as soon as possible after it is submitted to
our office.
JB/ds/ibm.21
• •
2 November 1988
TO: File
FROM: Jack Butler
SUBJECT: Telephone conversation with Roger Coats, Channel Master,
(919-93409711), NCD122263825
Mr. Coats contacted our office on this date to update the
subject project. The concrete pipe and sump to the east of the
concrete waste oil (septic) tank have been excavated and are being
stored on site. Sampling of the excavated area next to the building
shows a maximum of 18,000 ppb tetrachlorethylene and 230 ppb
trichloroethylene. A 3 to 4 ft. deep and 3 ft. wide ditch was dug
where the pipe had been. Sampling in this ditch revealed a maximum
of 280 ppb trichloroethylene and 190 ppb trans-1,2-dichlorethylene in
the end of the ditch nearest to the building. The second highest
levels were found at the discharge end of the ditch where 79 ppb
tetrachlorethylene and 54 pbb trichlorethylene were found.
JB/ds/ibm.46
~Channel • • ~a.I Master"' D1v1s10N oF AVNET I NC. • P 0. BOX 1416 • INDUSTRIAL PARK DRIVE, SMITHFIELD, N.C. 27577
May 2, 1988
Mr. Jack Butler
NC Dept of Human Resources
Division of Health Services
Solid & Hazardous Waste
Management Branch
CERCLA Section
P. 0. Box 2091
Raleigh, NC 27602-2091
Dear Mr. Butler:
Enclosed are copies of manifests for transportation of con-
taminated subsoils from our Oxford facility to the GSX land-
fill in Pinewood, SC Manifest No. 761 was the last load
transported as of this date. Channel Master was informed by
GSX on April 27, 1988, that they were approaching their an-
nual permitted volume limitation for their Pinewood, SC fa-
cility and that no additional contaminated subsoils could be
transported for disposal from Channel Master's Oxford facil-
ity until after July 1, 1988. Therefore all transportation
and disposal activities are on hold until July 1, 1988.
I have also enclosed for your file the total chromium analy-
sis for quadrants 1 & 2 and a sample point location drawing
with plotted concentration levels.
If you have any questions or need additional information,
please contact me at 934-9711.
Sincerely,
CHANNEL MASTER
Division of Avnet , Inc .
Roger L. Coats
Safety/Environmental Engineer
RLC/sc
Enclosures
cc: Charles Hansen
AN INDUSTRY LEADER SINCE 1949 • TELEPHONE [phone] • FAX 919-934·0380
SOUTHE.EST I NG AN.D PESEAl?CH L.ABrA·oF: I ES,
P.O. BOX 1849 -607 PARK AVENUE -~ON, NC
PHONE [phone]
ENVIRONMENTAL ANALYSIS REPOPT
DATE OF l?EPOF.:T:
DATE l?ECE I VED :
INC.
27H'33
BB/02/03
(38/01/25
F.:OGEF.: COATS
CHANNEL MASTEi?
P.O. BOX 1416
ACCOUNT NO.: 12f:,(J()
(OXFOF.:Dl
VOLATILE PESIDUE
NONFILT. F.:ESIDIJE
DISSOLVED PESIDIJE
UNITS
Cmg/U
Crnc:1/I..)
(rng/L)
(rng/Ll
(mg/Ll
(rng/U
(mg/1..l
Crng/U
(m,:1/l.)
(mg/U
Cms1/L)
(rng/U
(mg/I_)
(mg/Ll
Cmg/Ll
Cm,,/1..l
Cmg/l.)
(m,;1/l.l
( mg /1.. l
(mo/L)
(Y/Nl
3.00
y
TELEPHONE
B: WATEF.:
D:
B: 217C22
.87
y
''QUALITY SERVICE AT A FAIR F'PICE''
C: D:
._} ,r·;
"l:,
' ,;]1 ,l•r.••,it/
'•'·
-----,_.
J
'I
'.:); •·' ~: ''"· , ..
:~ .,.
SOI../THl,".rEST I l~G /\ND F:EHEM,:Cl·I LAE<□--□fc: I ES, I ~IC.
P.O. BOX 1849 -507 PARK AVENUE -W~ON, NC 27893
PHONE C919l 237-4175
ENVIRONMENTAL ANALYSIS REPORT
SAMPLE/TEST NO.---------> A: 217C21 B: 217C22 C::
MI Cf?OB I OLOG I CAL
COL I FOF:M, FECAL
COL I FOF:M, TOT AL
ANALYclEH
C:/lOOrnll
(CFU/lOOml)
----OTHER ANALYSES---~------------
:
COMMENTS:
.LAB USE ONLY-----------
ANALYSTs: NS
PICKUP: F:UHH:
·TIME: 5 HF:!3.Mll..ES: 140:
T: D:
I :
l?evie\.JP.d and Apj:)rovf2d _ 0
) ··1 ·f" f ,. :1 Cl' 1···1·· [71 t:' 'f /.:> ,.L:. lkY ~ 1::1m, ..•... ) ..
Manager, Enviror1mental Dept.
PAGE 2 •~f 2
D:
f:ilJUTl-11.:T._E,n I I\IEi (1~ID fi:[b[r,1:::c::1-1 I __ Arrn.or:: I Ee,, I NC.
P.O. BIJX 1849 -607 PARK AVENUE -WILSON, NC 27893
PHONE [phone]
ENVIRONMENTAL ANALYSIS REPORT PAl3E 1 ,:,f 2
LAB SAMPLE NO. (sl: 217C5-8
RECEIVED FF:OM
NAM
OR'G
ADD
csz
F:OGEP COATS
CHANNEL MASTER (OXFORD)
P. 0. BOX 1416
SMITHFIELD, NC 27577
SAMPLE(sl of: SOIL
MAF:f(ED A: 0-I 3 3 11
C: Q--I 4 ,..,,, c,
DATE OF REPORT: 88/02/03
DATE RECEIVED, 88/01/25
ACCOUNT NO.: 12600
ri:,:Lc':l''HONE
o-
B : Q-I 3 1 '::, 11
4
------SAMPLE/TEST NO.---------> A: 217C5 8: 217C6 C: 217C7 D: 217C8
ANALYSIS UNITS -------- ------------------------
pH
TOTAL RESIDUE
TOTAL VOLATILE RESIDUE
TOTAL NONFILT. RESIDUE
TOTAL DISSOLVED RESIDUE
BOD
COD
AMMONIA AS N
TOTAL KJELDAHL NITROGEN
NITRATE AS N
TOTAL PHOSPHATE ASP
CHLORIDE AS Cl
OIL 8, 13F:EASE
CYANIDE, TOTAL
(1110/I __ )
(mo/L)
(m9/U
(111[1/Ll
(m[J/Ll
(m9/L)
C:ni9/L.)
( lll\J /L)
(mg/l._)
(mu /U
(mg/L.)
(m£:1/L.)
(mg/Ll
------------METALS---------------
ARSENIC
·sELENIUM
CADMIUM
CHF:OMIUM
COPPEF.:
LEAD
NICKEL
ZINC
MERCUF:Y
SAMPLE DI 13EST I ON
vl/88
(111,;1/Ll
( mu /L)
(111,;1/l_)
(1110/1.._:,
(m9/Ll
(m9/l..l
(111£;1/L.)
(mg/L.)
(msi/l...l
(Y/Nl
54. ~30 D.50 875.00
y y y y
. r SOUTH~•rE~T I NI~ -'.\ND r,:~SE,,\~CH -LABo.:rn;: I l~S ~-I NC .
P.LJ. uux 184J -LU7 PAF~ AV~NU~ -w._~uN, NL 27893
PHCJNC (·:11·::,:, ::2::37 .... ,117:5
ENVIRONMENTAL AN~LYSIS REPORT F'AGE 2 of 2
SAMPLE/TEST NO.---------> A: 217C5 8: 217C6 C: 217C7 D: 217CB
MICROBIOLOGICAL ANALYSES -----------------------------
COL I FOF:M, FECAL
COL I FOF:M, TOT AL.
(1100ml:,
(CFLJ/lOOrnl)
----OTHER ANALYSES----------------
COMMENTS:
LAB USE ONLY-----·------
ANALYSTs, NS
PICf<Uf"': F:LJSH:
TIME: 6 HRS.MILES: 1 ·-lO:
T: D:
I :
vl/88
Review~d ancJ Approved
Jeffrey □'Harn, ~.S.
Manager, Envir·on1nen·tal
'-/) 'J
Dept.
ENVIRONMENTAL ANALYSIS REPORT F·,,GE 1 cf 2
LAB SAMPLE NO. (sl: 217C1-4
RECEIVED FF:OM
NAM
ORl3
ADD
csz
F:OC;EI? COAT'.3
CHANNEL MASTER (OXFORD)
P. 0. BOX 141G
SMITHFIELD, NC 27577
SAMPLE(sl of: SOIL
MARKED A: Q-I 1 3"
C:: Q--I 2 3 11
DATE OF REPORT: 88/02/03
DATE RECEIVED: 08/01/25
T[cl._EPHIJNE
B: Q-I 1 12"
D: Q-I 2 1 ·-::•11
------SAMPLE/TEST NO.----------> A: 217C1 8: 217C2 C: 217C3 D: 217C4
ANALYSIS UNITS ---------------------------------
. pH
TOT AL F:ES I DUE
TOTAL VOLATILE RESIDUE
TOTAL NONFILT. RESIDUE
TOTAL DISSOLVED RESIDUE
BOD
COD
AMMONIA AS N
TOTAL KJELDAHL NITROGEN
NITF:ATE AS N
TOTAL PHOSPHATE ASP
CHLOF:IDE AS Cl
0 IL ~, GF.:EASE
CYANIDE, TOT1,I._
(mg/Ll
(m9/LJ
(mu/Ll
(m9/I __ J
( 1119 /1..)
C m9 /L l
(mu/L)
(mu11_:i
(mg/U
(1119/U
(m~1/L.)
C:mo/LJ
(m9/L_)
------------METALS---------------
ARSENIC (mg/Ll
SELENIUM (mg/Ll
CADMIUM (mg/LJ
CHROMIUM (mg/LJ
COPPER C:n,g/1..l
LEAD (mg/1..J
NICKEL
ZINC
MERCUF:Y
Cmu/Ll
(mL,-1/L)
(mu/t_:i
(Y/N)
18. 00 178.50
'{ y SAMF'LE DI 13EST I ON
vl/88 "QUALITY :,c:r;:vrcE AT A F,\IF: n::ICE"
33. (H) 3.00
y y
SOUTll[cl?.EDT I NG AND RESl~AF::CH • L1\80I.CJF: I ES, I NC.
F'. u. oux'llllll!'/'."1,1.·) ..... c,o;• 1••·r,1:::1< AVE1,1uE: ... W _ .,ON, 1,1c: :::0 70·:)3
PHONE [phone]
ENVIRONMENTAL ANALYSIS REPORT F'r'\(:iE 2 of 2
SAMPLE/TEST NO.------· .. A: 217Cl 8: ~1,~£ C: 217C3 D: 217C4
MICROBIOLOGICAL ANALYSES
COLIF0F:M, FECAL
COL I FOF:M, TCJT 1\L
(/lOOml)
(CFU/IOOml l
----OTHER ANALYSES-------------..
COMMENTS:
LAB USE mlLY--
ANAL YSTs: NS
PIO'.UF": F:LJ'3H:
TIME: 6 Hl~:S.MIU:S: 140:
T: D:
I :
l?E':'V:i.E•WE\d dncl t~pprc:1VE.1cl l-10 ~
Jeffrey □'liam, p.s.
ManGge1~, Envi1~onmen·tal Dept.
vl/88 "/_;ILJALITY 8F,:l?'vICE AT ,~ r,\II~ c-'l?ICE"
ENVIRONMENTAL ANALYSIS REPORT 1°'Al3E 1 of 2
LAB SAMPLE NO. (sl: 217C9-12
RECEIVED FF:OM
F:013EC:: C!J1H:; NAM
ORG
ADD csz
CHANNEL MASTER (OXFORD)
F·. O. BOX 1415
SMITHFIELD, NC 27577
SAMPLE(sl ,:,f: SOIL
MAF:KED A: Q--I r.:.-'""'I II ....! .::,
C: Q-I I 1 1 •-::• II
------SAMPLE/TEST N□.---
ANt,L VS I 3
pH
TOTAL F:ESIDUE
TOTAL VOLATILE F:ESIDUE
TOTAL NONFILT. F:ESIDUE
TOTAL DISSOLVED RESIDUE
BOD
COD
AMMONIA AS N
TOTAL KJELDAHL NITF:OGEN
NITRATE AS N
TOTAL PHOSPHATE ASP
CHLORIDE 1\:3 Cl
0 IL ~, 13F:EASEc
CYANIDE, TOT1,L_
Ul.,l I TU
(mg/1..l
( ITICJ /1 ... )
(m':;;1/L_)
Cmci /U
(m~1/l ... l
(mq/1 .... )
(m9/I.._)
(rnu/L_:i
(rn<;1/l_l
(mt:;1/L)
(mci/L_)
(mull_)
(mu/l._)
------------METAL'.3---------------
ARSENIC
SELENIUM
CADMIUM
CHFWMIUM
COPF'EF.:
LEAD
NICKEL
ZINC
MEF:CUF.:Y
(rnu/1 __ :i
(rn9/L..)
C:rn9/L)
(m9/L)
C:m9/L)
(m9/I_)
(m~J/L)
(m,;i/L)
(mg/L_)
A: :217C'J
y
DATE OF REPORT: 88/02/03
DATE RECEIVED: 88/01/25
ACCOUNT NO.: 12500
Tl:LEF'HONE
E<: Q---I
D: D-I I
5 12"
1
E<: 217C10 C: :217Cl:I. D: 217C12
16.50 7.50
y y SAMPLE DIGESTION
vl/88 ''C'UAL.lTY f:if:F:VIC:C AT(\ r--·Arr::: f::•F:ICE''
SOLJTl .. ll~F--l~:3T I l\li;i AND l?E:UEA~'.CH L..AB(J.OF'. l E:3, I NC.
P.O. B□X~l49 -607 PARK AVENUE -W~□N, NC 27893
PHONE [phone]
MI CF':08 I □LOG I C1\L
COL I FOF;M, r-TCAL
COL I FOPM, TOT 1\L_
ENVIRONMENTAL ANALYSIS REPORT PAGE 2 of 2
(/lOOcnll
(CFU/lOOmll
E<: 217Cl0 C: 217C11 D: 2170::12
----OTHEP ANALYSES--------
COMMENTS:
LAB USE ONLY-----
ANAL YSTs: ~IS
PI CKUF': F'.IJciH:
TIME: 6 HPS.MILES:
T: D:
I :
vl/88
1.:1-0:
Reviewe1J anci Approved
Jeffrey D'Ham, 9.s.
Manager, Envirc1nmer1tal
'n" 7 ,,)
Dept.
. ,
...,,,
_s□UTHtcl.rE?T I N(i ., 1\~jl~ F:E:SE1\F:CH .... LABf~:CJI? I 1:::,, ~-
F. U. HOX 1 EM cJ .... tc,U 7 I· ,\kk ,<\V[,NLIL:c ..... wffl'.,fJN, 1,11_.
INC.
PHLINE [phone]
ENVIRONMENTAL ANALYSIS REPORT F'Al3E 1 of 2
LAB SAMPLE NO. (sl: 217C17-20
RECEIVED FF:OM
F:013EF: COATc: NAM
ORl3
ADD
CHANNEL MASTER (OXFORD)
F·. 0. DOX l.4lG
CSZ SMITHFIELD, NC 27577
SAMPLE(sl of: SOIL
MAF:KED A: Q-I I .:=I 1 ·-::, II
C: Q-I I 5 1211
------SAMPLE/TEST NO.---
ANALYSIS
pH
TOTAL F:ES I DUE
TOTAL VOLATILE RESIDUE
TOTAL NONFILT. RESIDUE
TOTAL DISSOLVED RESIDUE
BOD
· COD
AMMONIA AS N
TOTAL IUELDAHL NITF:C113EN
NITRATE AS N
TOTAL PHOSPHATE ASP
CHLOF: I DE AS Cl
OIL ~, GF:EASE
CYANIDE, TOT1\L
Ul'•.IITS
(mu/L")
(/THJ/L.)
(rngil)
(m9/Ll
(m9/L)
(rnu/1.._)
(rnu/L_)
(mo/L)
(mo/I._)
(m[[/l.l
(m,:i/L_)
(mtJ/! __ )
(msi/1_)
------------METALS---------------
ARSENIC (mo/L)
SELENIUM (mg/Ll
CADMIUM (mo/L)
CHF.:OM I UM
COPPEF:
LEAD
NICKEL
ZINC
MEF:CUF:Y
SAMPLE DIGESTION
vl/88
(mg/l_)
(mu/I._)
(m<J/Ll
<:mu/Ll
(m9/L)
Cm(J/L.l
(Y/Nl
DATE OF REPORT: 88/02/03
DATE RECEIVED: 88/01/25
ACCOUNT NO.: 12GOO
TEL.EF'HONE
El: Q--II 4 3 11
t::~ ,-. II , • .! ,:.i
A: 217C17 B: 217C18 C: 217Cl9 D: 217C20
4D::S. 00 275.00 380.00
y y y y
SAMF'L[/TCf:iT
MI CF.:08 I OL013 I C1'il..
COL I FOF.:M, FECAl.
COL I FOF.:M, TOT 1'il ..
ENVIRONMENTAL ANALYSIS REPORT
ND.--------A: 217C17 8: 217C18 C: 217C19
ANALYSES ------------------------
(/lOOml)
(C:f-"IJ/ 100ml)
----OTHER ANALYSES----------
COMMENTS:
LAB USE ONLY--------
ANALYSTs: NS
PICf<tJF·: F:IJS!-1:
TIME: E,
T:
HF.:S. MIU~S: 140:
D:
I : :
vl/88
f-?evi ewecl i::\ncl 1-:'\ppr eived 1 /-/Q
Jeffrey 0' 1-1;;:tm, .B. S. -1_7
Manager·, Env:iror1rner1·tal Dept.
F'Al3E 2 cf 2
D: 217C20
ENVIRONMENTAL ANALYSIS REPORT PAGE 1 of 2
LAB SAMPLE NO. (sl: 217C13-16
RECEIVED FROM
NAM
ORG
ADD
csz
F:013EF: COATS
CHANNEL MASTER (OXFORD)
F·. O. BOX l41C
SMITHFIELD, NC 27577
SAMPLE(sl of: SOTL
MAF.:f<ED A: Q--I I 2 12 11
C: Q-I I 1211
DATE OF REPORT: 88/02/03
DATE RECEIVED: 88/01/25
ACCOUNT NO.: 12600
Tl:.LEPI IONE
B: Q-II 2 3 11
D: D-I I ,.... ,...,,, ,:::, ,..:.,
------SAMPLE/TEST NO.-----A: 217C13 8: 217614 C: 217615 D: 217C16
ANALYSIS UNITS ---------------------------------
pH
TOTAL F.:ESIDUE
TOTAL VOLATILE RESIDUE
TOTAL NONFILT. F.:ESIDUE
TOTAL DISSOLVED RESIDUE
BOD
COD
AMMON I,; AS N
TOTAL f<JELDAHL NITROGEN
NITF.:ATE AS N
TOTAL PHOSPHATE AS F'
CHLOF:IDE AS Cl
OIL ~, GFEASE
CYANIDE, TOT1\I_
------------METALS-------
(mg/Ll
(rn~J/L.)
(m9/Ll
(mu /U
(mu/L_l
(m~;1/I....)
(mq/L_)
(mq/Ll
(mg/Ll
(m9/Ll
(mci/!_)
(mo/L)
(mci/1.._)
ARSENIC (mg/Ll
SELENIUM (rng/Ll
CADMIUM
CHF:OM I UM
COPPEf?
LEAD
NICKEL
ZINC
MEF.:CUF.:Y
SAMF'LE DI IJE,3T I IJN
vl/88
(H19/I __ )
(rncJ/U
C:m9/Ll
(m9/l...l
(rnc:;1/l..l
(rn9/L.)
(niq/L)
(Y/1\/)
64.50 l'JO. 00
y y
1o~t. oo
" '
33.00
y
EN\! IRUNlvlFl~TAL ANAL Y'.3 I '.3 li:[l'IJF:'T' F'AGE 2 of 2
SAMPLE/TEST NO.-------
MI CF::OB I OLOIJ I CAL_
COLI FOF.:M, FECAL
COL I FOF:M, TOT l,L
( / :!. 00ml)
(CFU/lOOml)
----OTHER ANALYSES---------------
COMMENTS:
LAB USE ONLY-----------
ANAL YSTs: l~S
PICKUP: nmH,
TIME: E, 1· .. ll?S.MIL[EJ: 1•-lO:
T: D:
I :
vl/88
Reviewed and Approver! •n" ··::, ... ,. ·•; , .. ·-. ' ("'' . J,,.,ffl <cy Cl IL,m, f, .. ,.,. c)
Manage1r, Environniental Dept.
j
j
' l ,
:
i
i
N
PROJECT
Channel Master
Oxford, N.C.
I
Test Plt locatlone
X
)(
X
e H-5 X
--
II ----
I
X III
Pie 4
X
IV
X
■ Pie I
--------
EffJ' \
\
X
\ .·
\
\
\
\
\
\
I
I
I
I
I
/
i _ Sample Locations
Concrete
30 , SCALE:t"•n rox.
JOB NO:osS-85-1398
FIG NO: I
CM-4 0
Influen
.
I
r:1,;
)(.
Exist
/
/
•✓ /
Tc~t Pit locnt 1011n
/
/
•
/
/
/
/ 1'6·,; ,,. l x
,>---...... ____ _
,,. -...
,,. X '-.. ,,. ' / '
/ ' /. '
/ \
/ ' .,, ■· Pit ) / X '
)( III X
Pit 4
X
X CM-2/ ___ _ • t 2
I
IV • M-5 X X
■ ?it I
'I-
/4on (o'-i.e; 'I----_ ..... -
Effl 1ent ' ' \ . •.
\
\
\
\
\
.\
I
I
I
I
X I
/ .,.,.
/
/
II X _ Sacple Locatio~s
'I-
1fl,; )(
/Dif
; '1 t;'
Concrete
I
'." .. ,. : .. ~ ~ . ._ 'i-tt;~ :· .. '
/::; · l:;_~--~~---.
·1~:::-~ .
, "• , "'I : ,.
• •
Comment.:; EQL -BELCl'v'./ QIJ?':NT!TATlOM L! t·,HT
Purgeob le Aromoti cs
! EA S3mple ·Mo. 350016 =
S~mple lrlentificolion O~<ford Pt·i:11:·e:3•:;ed
Date !\nal gzed ,_lulu 25 19l:i8 B~ f;,;ileu
s
7
Comoound
E1enzene
Ch 1 orot,en:ene
1 _.2-Di cf·i l or-ot;enzene
1,3-Dichlornbenzene
1,4-Dic!·11orobenzene
ct 1··1 ,1t,,c,•·,7p•·,,c, L.-. 1.j' _./,,__,J,_,
Toluene
1.0
1.0
1.0
1.0
1.0
1.0
1 _t)
Re~ults
Coni::entr~tion
u.g / l'.o
EiC!L
BOL
BQL
BDL
BOL
BDL
,; L
EilJL
• •
Comment:3 E:C!L -BELO\·V C!UP.Jff!TATIOM Llt···i!T
Purgecblc Hnlocorbons
I Er, Sampl~ No. 350016 2
Comoound
Chlorornet.hane
2 B r·o mo met ~11:: ne
.:1 \"1 n1J1 Chloride
4 [Jichloroditl u::ir·orr,?thane
6
7
10
11
12
13
1 4
15
i6
17
1:3
19
20
21
.... ,,-, .::.o
IM1,1!i(,ne chloride
T r·ic h1orni7 uoi-omethane
l _, 1 -Dii::!11oroet.tiene
1 _, 1-0ichlon:ieth:~ne
tr,:in.;;-1 _.2-Dii::!ilOr"oethene
Chloroform
112-Dichloroet.harie
1, 1, 1 -Trichloroethane
C,:irbon tetn:ichlor·ide
Bro modi ch Io rn met bane
1 , 2-Di 1:: h 11) ro p r-i:1 p::: ne
•::i::;-i _,3-Di•::hlor·opri:1pene
Trichlon:ie~hene
t.ran:3-l ,3-L-1ichl0r·opropene
1, 1 _,2-Trii::hloroeth;3f1B
ct,iorn,Ji brornorneth3ne
2-Chlor-oethiJ!vi niJl ether
81"0mc:for·m
T.~. t ra::: !1 !(1 r·o8t he ne
1, 1,2.,2-Tetr::ichl(1roethan~
Ch 1 o :-o tie nze ne
l )3-Dic.hlr:iiobcn:ene
1 _,2-Dich1ot·i:1be11z:ene
I ,4-Di c r11 on:, benzene
!3'J B2ileu
u.o/L
.0
n
.0
.0
0
.0
.0
I]
.D
.0
0
0
0
0
.0
.IJ
.0
.0
1.0
1.0
.0
.0
.0
.0
.0
.0
1.0
Re3ult~
Cc•ncentrat.ion
uq/L
· BQL
BQL
BQL
BQL
OQL
E:QL
BQL
BCtL •.
EaJL
B1JL
BQL
BQL
BQL
BQL
BQL
E,QL
i3QL
8QL
BOL
BQL
BOL
68
BQL
BQL
BQL
BQL ;
BQL
2
• FIELD S"4"1'LI~G IN'FORHATIONaIEET
CHAIN OF CUSTODY REC(9
(Hazardous ~aterials and Ochers)
~:on:: This form muse be completed prior co processing samples in Laboratory. (::o
samples will be processed withouc Job No. and Billing InscructionH:)
Client or
Laboratory Sample
(Lab Use Only)
No.: -----------
System Name: a ... ,,,~/ Mc,,,lg--------==-~~~=--------,------------
Councy: __ --=G"-''.,..'--'""'11--LIL.iLLll/..,_/z-=-----·---M~;/;,,,7r !!,,&/,.,,,: P.o, g,,I( /</It
Address : ___ _:.J-a,:---c.:.<.-"dS.>"'"""--'--{....--,'-"''"'=' -D=r..,,c.:' l/:..C<._-=-+--o_,_;e=-..::".:;.,--_,Cc1' ..,· µ;;..:..' t.:..·.:..• _____ ___;s;:;.;,,.,c... :.<.;J'-".j,C:..!-'(;.,_e /,_,,""/ u..,<...LC.:...S:"'--':...C. I
Date Collected : ___ 7._---'-/.,_1_-_.,f,_,._,f______ Time Collected : __ 2~•-' o_o_F-1?=½~-----'-(H-':-'-s'-.-'-)
Sample Location or Description: __ 9,,;~-!;.~-~o~r~c~/_· -~B~r_c_CA.~·~5~5_._e~,.f~· -1/~o_c __ c=o_½~h=c=-='~'u=,Jec=· =(~---
Type at Sar.1ple: 0 Water
If Hazardous: Dar or EPA ID No.:
[El' Or her .5o.' (
I Type Code (if any): _______ _ --------
Field Information/Comments (or) Samole Handling Precautions: _____________ _
I hereby certify that the above info~
1
ion i~ correct. ·
Collector's Certification: e::;;z:a ~ ~
, (Signature)
"Sample Allocation" and "Chain of Possession": (Sign & Date in Ink)
1. Sanple Collector: -
2. Sample Transporter:
J. Sanple Received in
4. Sar.iple Analysis Com
Signature
1Z~.~f~ /-,
~-7_~c:,c.0~<-~k°5-~.
\ Lab:
pleted:
Lab Test Reouested (List Below):
Lab Billing Instruction:
Date
7-/yr,{-j?
°t\ -,,~ r« l-l _.__
T ir.,e (Hrs.)
'·
--------------------------------
Spedal Instructions or Comments: ---------------------------
f I
;,;: 919 460 Oi !EA
rn Industrial & Environmental Analysr-s, Inc.
P.O. Gox 12546 • r-eseorch Triangle Porl,, NC 2·1709 • 919•46 7-9919
D&le: Octobftr 6, 1988
Roqe r Coll te
Chennel M&eter
P.O. Box 1416
Smithfield, NC 27577
Reference: I EA Reporl No. 350020
Deer Mr. Coele,
Tren&mltled herevilh ore 'the re3ult~ of enel y3es on lhrce Mmplee ~ubmttt~ to our
leboretory on S<lptember 30, 1988.
Pl~~ the enclo3e1'.1 report3 for 1/0Ur roeulb.
0 I
i
10dJ7/88 13: 10 2i: 919 460 0948 • •
Comment, BQL -BELOW OUANTITATION LIMIT
Purgeoble Holoc11rbons
EPA Net hod 60 I Compounds
. I EA Semple No. 350020 .1.
sample ldenttflcetion Sample 1
Oete Analyzed October 4 1988 By Curry
I EA
Soil
Nvmber Compound Ou,ntilation Limit
Jl.ill&.
1 Chloromethene 1.0
2 Bromomethene 1.0
3 Vinyl Chloride 1.0
4 Dichlorodifl uoromethane 1,0
5 Chloroethene 1.0
6 Methylene chloride 1.0
7 T richlorofl uoromethane 1.0
8 1, 1-Dichloroethene 1,0
9 I, 1-Dichloroethene 1.0
IIJ trans-1,2-Dichloroethene 1.0
11 Chloroform 1.0
12 1,2-Dichloroethane 1.0
1 3 1, 1, 1-Trlchloroethsne 1.0
14 Cerbon tetrechloride 1.0
15 Bromodichl oromet hsne 1.0
16 1,2-Dlchlorop1·opane 1.0
17 tran,-1,3-Dichloropi-opene 1.0
. 18 Trichloroethene 1.0
19 ci,-1,3-Dichloropropcne 1.0
20 1, 1,2-Trichloroethane 1.0
21 Chlorodi bromomethene I .0
2.2 2-Chloroeth,Jlvi nyl ether 1.0
23 Bromoform 1.0
24 Tetrechloroethene 1.0
25 1, 1,2,2-Tetrechloroethana 1.0
26 Chlorobenzene I ,(I
27 1,3-Dichlorobenzene 1.0 . 26 1,2-Dichlorobenzene 1.0 29 1 ,4-Dichlo'robenzene 1.0
03
Reaults
Co nee nt rot i,ir,
l\.Q.L!]_
BQL
8QL
BOL
BQL
BQL
20
16
EJOL .
BQL
BOL
BQL
BQL
BQL
BOL
BQL
BOL
BQL
4
BOL
BQL
BQL
BQL
BCIL
BOL
BQL
13QL
BQL
BQL
BQL
Z: 919 460 0948
Comment3 / BQL -BELOW QUANTITATION Llt11T
N/R-Nol Reque,ted
•
-------__ , ____ J
Purge11ble Arom11lics
CDA Mothl':I,_. ,:.r.'J rnnr1nn11nrl,-,. L.O o-, 1 ,._,. ._ffVU U'V".E.. \...,O•••J-'UUIIUJ
I EA Semple No. 350020 l
Sample Identification 3ample I
Date Analyled October· 4 1988
Number Compour,d
Benzene
2 Ch I 0I·obenzerre
3 I ,2-DicI1loroDenzene
4 1,3-Di chlorobenzene
" 1,4-Dicli 1 orobenzene J
6 Ethyl benzene
7 T,)luene
B Tot.I'll >:qlenes
\''ioler ✓-~oi I
011anti tAtion
llmit
~
1.0
1.0
I.Cl
1.(1
1.0
I 1)
1.0
M/R
02
Re~ults • ,.
Concentr-et1~r,
~
., ...
BOL
BIJL
flOL
BOL
BOL ,., -
' '
Z. 919 460 0948 • •
Comments BQL -BELOW QUANTITATION LIMIT
Purgeoble Holocorbons
EPA MethQd 601 Compounds
I Eli Simple No. 350020 £
:lemple ld~ntlflcalion Sample "2
Date Anal vzed October 4 t 988 BIJ Curry
!EA
Weter
Number Compound Ouanlitation Limit
illill.
1 Chloromethene 1,0
2 Br~momethsne 1.0
3 Vi r,yt Chloride I IJ
4 Dichlorodifluoromelhane 1.0 s Chloroen,ane 1.0
6 Methylene chloride 1.0
7 Trichlorofl uoromethane 1.0
8 1, 1-Dlchloroethene I .0
9 1, 1-Dichloroethene 1.0
1 O tran~-1 ,Z-Dichloroethene 1.0
11 Chloroform 1.0
12 1,2-Dichloroethane 1.0
t 3 1, t, 1-Trichloroelhar,e 1.0
14 C8rbon telr8chloridr. 1.0
I 5 Bromodic.hloromethene t.O
16 1,2-Dlchloropropene 1.0
17 lrans-1,3-Dichloropropene 1.0
I 8 Trichloroettrene 1.0
t 9 cis-1,3-Dichloropropene 1.0
20 I, 1,2-TrichloroethAne 1.0
21 Chloroctl bromomethane 1.0 22 2 l'htoroethylvi nyl ether 1.0 23 Bromoform 1.0 24 Tetrachloroethene 1.0
25 1, 1,2,2-Tetrachloroethene 1.0
26 Chlorobenzene 1.0
27 1,3-Dichlorobenzene 1.0
26 1,2• Dichlorobenrnnc 1.0
29 1 ,4-Dichlorobenzene 1.0
05
Results t
Concentre1!(,r,
!!.ills
BOL
BQL
BOL
8QL
BOL
6
I
BQL
BQL
BQL
BQL
SOL
BQ.L
BQL
BQL
BOL
BQL
BOL
BQL
BQL
flQL
BQL
BQL
BOL
BQL
BOL
BOL
BQL
BOL
2i: '~19 4t,O 0948 •
Commenb BQL • BELOW Ol!ANT/TATION Lll11T
N/R· N(,t Req11e,ted.
•
Purgeoble Aromolics
F.PA Method 602 Compounds
IEA Sample No. 350020 £
Sampl11 Identification Semple 2
Date Anal gzed October 4, 1968
Im
$,)11
Quent\t.etior,
Number Compound Lrn11t
ill&
1 Benzene 1.(1
2 l1,: ~ :·abenzene 1.0
3 1,2-Dich 1 orobenzene 1.0
4 1,3-Dichlorobenzene 1.0
5 1,4-Di chl orobenzene 1.0
6 Ethyl benzene 1.0
7 Toluene 1.0
B Tote! Xylenes N/R
04
Re,ulh ..
1;0 nc~ nt r"Bti o ii
ill&
BOL
BOL
BOL
BOL
BOL
BOL
BQL
1'
~ 91'3 460 0948 IEA • •
Commen\5 BQL -BELOW QUANTITATION LI MIT
Telrechloroethylene end I, 1,2,2-TelrachlorMtr,ane coelute
GC/MS analysfa is r~commerrded frlr confirmation.
Purge ob I e lfo I ocorbons
[PA Method 60 I Compounds
I EA Sample Nn. 350020 ~
Se111ple Identification Sample 3
Date Anel 9zed October 4 1988 By Curry_
Soil
Num~er Compound Quantitation Limit
billfil.
1 Chloromethane 1.0
2 Bromomethane 1.0 .. Vi ny1 Chloride 1.0
4 DichlorodiO uorometMne 1.0
5 Chloroethene 1.0 6 Methylene chloride 1,0 7 T richloron uoromethane 10
8 I, 1-Dichloroelhene 1.0
9 1, 1-Dichloroelhane 1.0
10 treM-1,2-Dictilor·oeth-,ne 1.0
11 Chloroform 1.0
12 1,2-Dichloroelhane 1.0
13 1, 1, 1 -Trichloroethane 1.0 14 Carbon t_etrachloride 1.0 15 B romodi c hloro me! ha ne 1.0 16 1,2-Dichloropr;opane 1.0 17 traM-1,3-Dichloropropene 1.0
18 T rich 1 oroet hene 1.0 19 cb-1,3-Dichloropropene 10
20 1, 1,2-Trichloroethane 1.0
21 Chlorodi bromomett1ane 1.0
22 2-Chloroelhylvinyl ether 1.0 23 Bromoform 1.0
24 Tet rec hloroet he ne 1.0 25 1, 1,2,2-Telrachloroe\hane 1 0 26 Chlorobenzene 1.0
27 1,3· Dichlorobenzene 1.0 28 1,Z·Dichlorobenzene 1.0 29 1 .4-D1ch1orobenzene 1.0
Reau119
Concentration
~
BQL
BOL
BQL
BQL
BQL
14
3 sol
BQL
BQL
BQL
BOL
BQL
BQL
BQL
OOL
BOL ,
BQL
BQL
BQL
SOL
BQL
1'
BQL • -
SOL
BQL
BOL
8QL
• •
Comment, SOL -BELOW QUANTITATION Lll11T
N/R • Not Reque~\e,d
1 E\'.l •
Purgeoble Arom11tics
EPA Method 602 Compounds
I EA Sample No. 350020 .1
Sample ldcntificotion Sample 3
Date Analy;,:ed October 4 1988
Nymber Compound
Benzene
2 ' Ch 1 orobenzene
-, 1,2-Di ch 1 ornbenzene .,
4 1 ,3-Di ch I ornbenzene
s I ,4-Di ch I orobenzene
6 Ethyl benzene
7 Toluene '
B Tot.al Xylenes
By Curr1J
Weter/Soil
Ou~ntitation
. Li rr,11
!!&Tu
1 ()
1.0
1 .(1
1.0
1.0
1.0
1.0
i-1/R
07
Results.
~oncentratioh
ugn'.g
BOL
BOL
BOL
BOL
BQL
I
•
Comments QNR= Quantitation Not Requested
Tent11tively Identified Compounds
IEA Semple ID: 350012 .?..
Client Sample ID: Fill Dir!
Applicable Fraction: Yolatile!X:J Bose/Neutral I I l\cidl I Other! I
Tentatively Identified Compounds (TIC) refer:, to substances not pr·esent in the list of target compounds.
Therefor-e, not all TIC's are identified and quantitated u,,ing individual standat·ds. TIC li,,tings are prepared
utilizing a computerized library search of electron i mr,act mass spectral ,Jata and evaluation of the
relevant data b•J a mass spectral data specialist.
Quantitation is accomplished by relative peak t,ei•Jhl of the compound compared tot.Mt of H,e nearest
interr,;,l standard from the total ion chromatogram. TIC's are identiiied and quantitale,J onl•J if_H,e pear:
height is I O % or mo r·e of lhal of I he nea r·esl i nle ma l sta ndc; r·d.
TIC i"!11me Concentr11t ion µq/Kq
None found es per ebove cr·iteri e ONR
.;
: ; Comnients: IlQL = Ilelow Quantitation •'----------, rn
· B = Compound in Blank
CLP Volalile Deliverables
350-12-2 TEA Sample No.
Sample I.D.
Date Analyzed
Fill Dirt
5117/88
Volatiles
1. Chloromethane
2. Bromomethane
3. Vinyl Chloride
4. Chloroethane
5. Methylene Chloride
6. Acetone
7. Carbon Disulfide
8. l1!1Dichloroethene
9. 1. 1-Dichloroethane
IO 1,2-Dichloroethene (Total)
11. Chlorofonn
12. I 12-D1chlorocthane
13. 2-Butanone
17. Bromodichloromethane
18. 1.1.2.2-Jc1rachloroc1lrnne
19. 1,2-Dichloropropane
20. trans-1,3-Dichloropropene
21. Trichloroethcne
22. Dihro111ochloro111cthane
23. I, 1,2-Trichioroethane
24. Benzene
25. cis-1 J-Dichloropropene
26. Bromofom,
27. 2-1-lcxanone
28. 4-Methyl-2-pentanone
29. Tetrachloroethene
30. Toluene
31. Chlorobenzene
32. E1hyl Benzene
,4 Xylcncs CTornl)
Ily Q'TooJe
Quantitation Limit . (µg/kg)
JO
IO
s
10
5 s
5 s
5
5
10
5
5
s
5
5
5
5
5
5
5
10
10
5
5
5
5
5
5
Concentration
(µg/kg)
BQL
BOL
BOL
BOL
BOL BQL t
BOL
BOL BOL B()L
BOL
BOL BOL
BOL
BOL
BOL
13OL
BOL
BOL
BOL
BOL
BOL BOL BOL
ll()L
no1,
\''• · .. ..... '' '', ,/ 2' ',,! " ~
..
'
·• ~ Industrial & Environmental Analysts, Inc.
P.O. [3ox 12846•P-eseorch Triangle Porl~. NC27709•919-467-9919
Date: September 15, 1938
Roger Coats
Channel Master
P.O. Box 1416
Smithfield, NC 27577
Reference: I EA Report No. 350019
Dear Mr. Coats,
Transmitted herewith are the results of analyses on eiiJhl samples submitted lo our
laboratory on September 8, 1988.
Please se-, the enclosed reports for your results.
Very lrul•J yours,
INDUSTRIAL & ENVIRONMENTAL ANALYSTS, INC. ~ ~£'~----z~~ ~~k Randall
Senior Chemist
Offices and lobororories locored in: Essex Junction, Vermont
P.eseorch Triangle Porl\ North Carolina
• •
Comments BOL -BELOV·l QUt,NTITAT/Ot·I LII .. IIT
'
I EA Sample No_ 350019
PurgeHble HHlocarbons
l
Sample Identification Area 1-Side Slope
Date Analyzed September 12. l98~:
Nurnber ComDound
Chlo1-or11ethane
2 Bn:irnomethane
~ Vi n•Jl Chloride -· 4 Dichlorodifl uor-omethane
5 Ch 1 o roe!. ha ne
6 Meth1Jlene chloride
7 T richloro!l uoromethane
8 1 .• 1-Dichloroethene
9 1, 1-Dichloroethane
10 tr-an,,-I .,2-DicrilonJetr,ene
11 Chloroform
12 1,2-Dichlor'oeH,;;ne
13 1, 1, i -Tt'ichlon:,etr,ane
14 C;;r·bon 1.elHchloride
15 8 r·omodi ch loro methane
' 16 I ,2-Dichlor-opropanB
17 tr-en,,-1,3-[1ich101·opropene
18 Trichloroethene
19 ci,-1 ,3-Dichloropropene
20 1., ~ .,2-Trichloroethane ,., .
<. I Crrlot•octi t,rornometr,,ine
22 2-ChloroethtJlvi n1::11 ether
23 Brornofor m
24 T et rac tr1 o roet. r,ene
25 1, I _,2,2-Tetrachlc,r·oethane
26 Ch 1 (•ro t,e nze rre
27 1,3-Dichlorobenzene
r,~ i.Q 1,2-Di(:hlorobenzene
29 1 ,4-Dichlorobenzene
By Baileq
Results
iJuantiteti,,n Limit Co nee nt ration
p.q / f:~q ug/Kq
1.0 BQL
1.0 BQL
1.0 BQL
1.0 E:QL
1.0 BQL
1.0 E,QL
1.0 BOL
1.0 E:QL
1.0 B!JL
1.0 80L
1.0 BOL
1.0 BQL
1.0 1
1.0 BQL
1.0 BQL
1.0 BOL
1.0 E:QL
1.0 BOL
1.0 BQL
1.0 BQL
1 0 BQL
1.0 SQL
1.0 BOL
10 BC!l
10 E:QL
1.0 E:QL
1.0 E:QL
1.0 . E:QL
1.0 E:CIL
j
. :.~··.?f:.: ~.
:-:: t/.·:: .. . -"'1·· ., ~-
·• . . ~ ... ~~::-: -.
/~,--:t )h~::
. ;/;.,....:,,, -·-··,. '• . ·--,. ·-....
'•• '• ; . ~-~ --. ·.-. ·':"•; .. ,,
--~~~ ;:1 --' . -. . '
)'.;
' -..... ,/ .... ,. · ... ',. --"s~-.:.. -~<-, l • • . , .. -· ·::~r·
• •
Comment, BCIL -BELO\"/ Cil_lAr-/TITATION LIMIT
Purgeoble Aromatics
!EA S8mplello. 350019 l
S8mple Identification At"B8 I -Side Sl0DB
Date /\nel yzed 5epti?.mt•et· 12, 19H8 Bg Beileq
R'esults
1./IJmbet· ComDoun1i Ouent.it.etion Limit Concent.r,:1tion
u.q/!:::q uq/~~q
Benzene .0 BCIL r, Ch l orot,enzene 0 Bt)L ,{_
,., 1,2-Di ch I cn-ot,enzene .0 BOL
4 1 "" "i r'11 -··1bi:>p~ · r -!._,-t..., -·' r,1-11 L _. ,.::.I:! I~ 0 BQL
5 I ,4-Di chi orobenzene .0 BOL
6 Etl·rqlt,enzene 1.0 BOL
7 Toluene () BQL '
0 '-' )(yl enes .0 BCIL
• FIELD S,l.c'PLI):G U!FOR!-l<\TION SHEET
CIIJ\1:1 OF CUSTODY RE.D
(Hazardous '.laterials and uthers)
~:or::: This fur.n ~ust be completed prior to rroccs!":inr, samples in L.1bor3co:-·/. (;:o
sa:nples tJill be processed without Job (!o. ,1.nd Billing Instructions.)
Job ~lo. : I'. 0. No. I, 0 I S 6 T..,horatory S.1rnplc '.lo.:
( L.1 I, Use Only)
Client or System Name: Channel Master
Count-,.: Johnston
Address: p.' 0. !lox 1416
Dace Collected: (c C-\ C] s· (.' Time Collected: ,~-' (:-l~s. . r-I I ,, '
Sa np le Lo·c a t ion or Des c rip t ion : _ __!l~'!!"~~~o:s.c:io1iJl:..Jf'_!r~o?_!n~•-V~CQ_l_leC_J;c!!o~nc!t~a!!n'!.:d\_i1"'rn!l!_t g_egd_i!aJ;r:;:euaL _____ _
at the Oxford NC Cleanu Site.
Type oC Sar.ipl~: 0 Water O Wastewater O Sluclcc O ll.1.zn.rdous W,,ste UL) Other Soi
If Ha:adous: Type Code (if any): ---------DOT or EPA ID tlo.: --------
Field Infonnat ion/Cormncnts (or) Snrnolc llandlin~_ Precautions: ____________ _
I hereby certify that the above i_pformation is_ correct,
1/-'l ;:' . ,, '
Collector's Certification: I 'r.(,/f-< ,_c /.-.,., -e}-·\ --...L'--'-'-'-'-'-'--'---="'----'-..:....----=--'-----------------------
( (Signature)
"Sa;;:yle Alloc.Jtion" and "Ch:1.in of Possession": (Sir,n & Date in Ink)
l.
2.
J.
1/ /
Sanple Collector: /t_;u_.1_1,u ( (;,_";,,c•--~, -~~~;---'--~---'--'-----------
Sar;ip le Transporter:
Sanple Received in -L-ab-:--/j-m--cM;,y--}!-_'j_ -1-.J:..-1 l;-,u'.ix,-,-I_ -,.-.J,l---_-_ ----t-(-/--'¼-, ---5--=\-1"1--/--2--,-,1..,-\~
S a.::1 p 1 e Ana 1 y s is Comp 1 e t_e_d..J:;,,.L"'--::,IJ+--.£;.====:...:..,==-------I..L--'--==--"----1,----''------
--,-------------------------------
Signature Dote
Lab Test Reottested (List llelow): Level I
Method 601/602
Lab 51llin5 Instruction: ---------------------------~------
j
.1·· •• '
·, ;, . ~ ~
·• ·~·, . '\:-:
;)r :._.
-:.·.!
•
Cornmer,\c3 BOL -8ELO'W' C!IJ,\NTIT/,TION LI IIIT
Purgeoble Holocorbons
IEA Sample Ho. 350019
Semple !d~ntification Ar·e3 1-/\dja,;ent to Fence
Date hnal yzed ::;eoternber 12 198:3
Murnber Cornnound
Chlo n)m>:.t ha ne
2 BromomeH13ne
3 Vi r!!Jl Ch1orid~
4 Dich1or·o,Ji17 uorometh;;ne
C ·-'
6
7
10
11
12
i3
14
15
16
l ,-, 10
19
20
21
23
24
29
Ct, 1 o met t,a ne
t·-·1eth1J1ene :::h1cride
Tr·ichloroll uororneth;;ne
1) 1-Dicifloroetllene
1 _, 1-Dichl•)r•)eth::ne
t ran.:;-1 . 2-Di c:t-il o n:11:!U-1e ne
Chloroform
1.,2-Dichioroettnne
11 11 i -Trichloroetr1ane
C::irbon tetree:tiloride
8 ro modi ch lo rornetha ne
1 .. 2-Di c ti lo ~-op r·o pant
tt-err~-1 _,.3-Dichlon:•propene
Tricllloroethene ·
ch-1 _,3-Dichloroprcipene
1 .. 1 .,2-Trichloroethane
Chlorodi bromornetl1ane.
2-Ch1oroethtJ1vin1Jl ether
Brornofot·rn
Tet rac h1 o roet he ne
1, 1 _,2_,2-Tetr8(-hli:1roE-.th:ane
C~1lorot1enzene
1 )3-Diehl orobenzene
I .,2-Dli::hlorobenzene
1 .4-Dici!lot·obenzene
By Beileq
ll.•J/1::q
i .0
1.0
1.0
I .Lr
1.0
i .0
10
1.0
1.0
1 _(I
' IJ 1.0
1.0
i.O
1.0
1.0
I . •:1
1.D
1.0
1.0
1 0
1.0
1.0
I .IJ
i .0
i .0
i .0
1.0
1.0
Results
u.qn~g
E:QL
t:C1L
BQL
8QL
E:QL
BQL
BQL
8QL
BIJL
BC!L
8QL
BOL
BCIL
BC!L
E:QL
E:Cll
E:IJL
E:C!L
BQL
E:QL
BQL
BQL
E:QL
BQL
E:QL
BQL
E:QL
BQL
. . ,
::, .tj '•~ -l.
(·.:-~ •.. -
. ' '
.. .
• •
Cc:rnrnent~; BQL -BELOV·f OUANT!TATIOI-J L!t·.-1JT
Purgeobl e Aromoti cs
I Ell Sample Ho. 350019
s~mple Identification Mee 1-Adiocer,t to fer,,:o,
Det~ l\nal •Jzed ·3~pf.ember 12, 1 '~188 Bl).
Nun-!t•~r
4
C ._I
6
7
6
Compour1d
Benzene
' Ch l or-otienzene
1,2-Di c:r·!l ornbenzene
1 .'3-D i c:!11 ::ir-1:1tienzene
1 . .4-Di ch 1 cwobenzene
Cjl·11l!--,---,-,-,-L .I!.~ t L!t!t J.::._!jJ Jf:!
Toluene
Ou3r,\i\8tion Li rnit
u.,1/l'.a
1.0
1.0
1.0
1.0
!.O
1.0
1.0
1.0
Results
Concentr·ation
U.•J /Ka
pr,1 I q" _ .......
BCll
BCIL
Bi)L
EiC1L
EiOL
,-,
L
•
FIELD SA.'n'LI):G UrFOR!-Lf\TION!!EET
C!IJ\ Pl o,· CUSTODY RECD
(Hazardous ~taterials and Ot 1ers)
1:or::: This iu,rm ::,use be completed prior co processing samples in LJboracoc,. c:o
sa:nples! will be processed without Job llo. nnd Billing Instructions.)
Jo.b '.lo.: P. O. No. 40156 L.1borntory S,,mple !lo.: -----------(Lab Use Only)
Cli~nt or Syscem Name: Channel Master --===--=~"'-"--------------------
County: Johnston --------------------
.Address: P.·o. Box 1416
Date Codected: (1:y;/J ;qs·~, Time Collected:_~/_,_/_(_'(_' ______ (~~~~~s..c...:..)
Sz::,ple ~ocation or Description:_~~!!!il!!!'!!'!!!!~s~o~illcJ'fir~o~m~V~O~Cc_<;c~o~nut~a~m~i~n~aut~e~cLl~aur~e~aL _____ _
at t~e Oxford, NC Cleanup Site.
Type oi Sar:,ple: 0 \.later O Wastewater O Sludge O llaza.rdous Waste lliJ Other Soil
If Hazardous: Type Code (if any): ---------DOT or EPA ID 1/o.: --------
Field Infor.nation/Comments (or) Samole Handling Precautions: --------------
I hueby certify that the above info~;;tivry .i~ correct, /, I ,. , /
Collector's Cartification: . C-C.•-'a r /!',-,.,·.,<..
1 (Signature)
"Sa;c?le Allocation" and "Chain of Possession":
Signature
1/
(Sign & Date in Ink)
Date
1. Sar.iple Collector: ( /1:/ 1.:/.c1 ( \, ,,if
2. Sar.ip le Transporter:
J. Sar.iple Received in Lab:
~ Sa.:aple Analysis
Lab Test Reauested (List Below): Level I
Method 601/602
Lab Silli~3 Instruction:
T::::e (:1cs.)
---------------------------------
i \ · ., :r ·
' -: ,-::.t ..
~~A: :J{· ~. -:·
'·' ',';:; .. ~· . -· ...
,•. .. '
• •
Commenh BQL -BELO'W QUANTITATIOI·/ LIM!T
Purgenble Hnlocnrbons
I EA Sample No. 350019
Sample Identification Area I -E:1Jild. 3ide 31,:,oe
Number
2
4
C ·-'
6 .,
Ci
9
10
11
12
13
14
15
16
17
. 1 g
19
20
21
23
24
25
26
27
Chlo ro methane
Bro mo met ~13 ne
Vinyl Chloride
Compound
Di c: h lo rodi t7 uo ro rnet h8 ne
Chioroethane
1··1dh1Jlene chloride
T 1·ichlo1·ot11Jornmethane
1., 1-Dictiior·oethene
1 _, 1-Dichl,:,1·,Jen,&ne
tranca-1,2-Dicr,loroethene
Chloroform
1 .,2-Dichloroethane
11 1, 1-Trich1oro13tr1ane
c.j r bo n td rac h lo t·i de
Bro modi ch lo ro methane
1 )-Dichloropropane
t.r-an,;-1,3-C•i,:,hioropropene
T 1·i,::hloroethene
ci:,-1,3-[iichlor·opropene
1, 1,2-Trichloroe\tm,e
Ctilorodi t,1·omomelf,3ne
2-Chloroeth11lvln1Jl ether
Bromofonn
Tet rac h lo roet he ne
1, 1,2.,2-Tetr3ch1orne\tm,e
Chlorobenzene
1,3-Dichl•:,robenzene
l _.2-Dichlorobenzene
1 .4-Dia,ior·ot,en.:ene
Bg Corn·•.-/e11
Ouantib:it.ion Li rnit
u.q/Kq
10
1.0
I.Ct
1.0
1.0
1.0
1.0
1.1)
1.0
1 0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.Ci
1 0
1.0
1.0
1.0
Results
Conc:entt·ation
~19/Kq
BOL
E:QL
BOL
BQL
BOL
BQL
BOL
BQL
80L
BQL
BQL
BQL
BOL
BQL
BOL
BQL
BOL
BQL
BQL
E:Ctl
BQL
BQL
BQL
E{tl
BOL
BQL
SOL
E:QL
5QL
.,.. ,.
. ,., ..; :
• •
Comment:, BCIL -BELOV{ QIJANTITATION LIMIT
Purgeeble Aromatics
I ff, Somple Ho. 350019 7 ·-'
Sample Identification Area 1 -Build. %Je Slope
D3!e Analyzed :3eptember 12, 1 %8 By Currq
Number
3
4
Benzene
Ch 1 ornt,enzene
1 ,2-Di ct·11 ornt,enzene
1,3-Di ct-11 orot,enzene
1 ,4-Di ci-1 ! orot,enzene
6 Ethyl benzene
7 Toluene
8 'JI 1J ·0 t·1a•·· ,", -:I t= ,_ .. :,
Results
Ouantitation Li mi1 Conc~ntration
uq/Kq uq/Kg
1.0
1 0 E,QL
10 BC!L
i.O BCIL
1.0 BCIL
10 BQL h 1 ,., I 1
1.0 r,
L
• FIELD SAHPLI:!G Ic!FOR.!-l<\TION.-1.IEET
CIIAI:l Or CUSTODY RECC9
(lfazardous ~latcri,115 .,ncl Otl,crS)
~:OTE: This fur.n :;tUSt be completed prior to processing sampli:!s in Labor.1co-:-:,·. C:o
:;a:nples will be processed wichouc Job Mo. ,1nd □illing Inscruccions,)
Joo '.lo.: r. o. Nn. 1,01sr, --------~~-------Laboratory Sample No.: ------------' (Lab Use Only)
Client or System Name: Channel Master -----'-==='-'-===------------------------
Count;·: ---------------------Johnston
Address: P.·o. Box 1416
Dace Collected: (r, s·,·p \'.]'?(1' Time Collected: 11 , ,·c..: (:ics.) -'--'--'----=---------'-'-'-'-;c..:...:.
Sanple Location or Description: _ _..'!!~~!"""'!""!~~s202illcJfjr~o~m~-~V~OQfC_..£c£D~J1~t~a~n~Ji~,~1a~. t~·c~cil_..i:!a~r~e~at_ ______ _
at the Oxford, NC Cleanup Site.
Type oi. Sar.ipl~: 0 Water O Wastewater O Sluclcc O Hazardous W,,ste [xJ Oche-r Soil
If Ha:ardous: Type Code (if any): ---------DOT or EPA ID No.: ~--------
Field lnformacion/Cornment5 (or) Samole llandlinG_ Precautions: ---------------
I hereby certify chat cl1e above information is correct, /} I .. · /
Collector's C.ertification: /.c!c, / _ _,,-. ( /i:,,j., ----'-''-""-"---+------'----c-------------------( Signature)
"Sa;;-;iJlc Allocation" nn<l 11Ch,1in of Possession": (Sir,n & Dace in Ink)
,,) .. / 3icna :.ure
l. Sar.iple Collector: \_.tvL,, (/(, .,',, ( ,,;·' i ! ,,·-c, --~~~-+--~-~~~~----------1---~-'----+---~~---
D.itc. T'.c:e (He,.)
2. Sar.iple Transporter: ----#'1--------~-~--~-----+-----'--------
J. Sanple Received in Lab: C -'3'~1 (c.t.J<..) ~=~~=---===-=-=--"...=..-=----1-"L-..;::_-==-+-1 -'------==---
k, Sa;aple Analysis Completed: --------------------------------
Lab Test Reouested (List Below): Level I
Method 601/602
Lab Silli~, Instruction: -----------------------------------
. .·; .. ~ .~ .,. , ,
·-:----:;. ~-
, .. ~: .
'• ·•' .. . .· ·,.) -
• •
Comments BQL -E,ELOVI'° QUAIHITATION LIMIT
Tetrachloroe\hylene ,ind 1 _, 1,2_,2-Tetrachloroe\h;;ne coel ute. GC/M:3
;J n;J l 1pi :i i :i t·eco rn rne n,je,J io r co nfi 1· rnati on.
Purgeoble Holocorbons
I El'\ Sample !fa. 350019 4
Sample Identification Ar·ea 1-Bo\l.om
Datp •nal nzPd ,o. itornhor· 1-; 1 c,oo ,..H ~ ~ .__'~j-1·.·-· ......... 1 .·UU By Cor-rr•,/ell
Number-Compound Ouantitation Limit
u.q/T,i
Chlorometh;;ne 1.0 c, Bro mo met h;; ne ' 1.0 '-
3 'ii n•Jl Chloride 1.0
4 Dichlorodi tl uorometh3ne 1.0
) Ch 1 o roi::.t ~1;:1 nB 1 0
6 t·-·1eth~lene chloride 1.0
/ T r-!chlornt7 uorornetharie 1.0
ti 1, 1 -()ich101·oethene 1.0
9 1, 1-Dichlori:,ethar,0 1.0
10 tt·an3-1,2-[1ichlot·oeH1ene LO
11 Chloroform 1 0
12 1 .2-Dicbloroethane 1.0
13 1, 1, 1 -Trichloroethane 1.0
14 Carbon !.et rfic h lo t·i de 1.0
15 Bro modi ch lo r-o methane 1.0
16 l ,2-Dichloropr-i:1p;:1ne 1.0
17 t.rans-1,3-Dichloropropene 1 Cr . ,_,
1 B Tri ch lo rnBt he ne 1.0
19 cb-1,3-Dichloropropene 1 0
20 l) i .,2-TrichloroeH1M1e 1.0
21 Chlon:11Ji bn,mometfF1ne 1.0 ·:,') .:...:.. 2-ChloroethiJlvi n!Jl ether 1.0 .-)7 Bt·omoform [._.J i .0
24 Tet rac l1l o rci~t lie ne 1.0 .., C: i, 1,2,2-Tett·achloroelh~ne 1.0 "'._!
26 Chlorot,enzene 1 0
27 1,3-Dichlorobenzene 1.0 ,,n LO 1 .. 2-Diehloroben2ene 1.0
29 I ,4-Di,;hl,not,enzene 1.0
Results
Concentration
ug/Kg
BQL
BOL
BOL
BQL
BOL
BQL
BQL
E,Od
BQL
3
BQL
BC!L
E,QL
BQL
BOL
BQL
BQL
46
SQL
BCIL
BQL
BQL
BQL
19
8QL
BQL
BQL
BQL
8QL
• •
Comments BQL -BELOVi QUANTITATION LIMIT
Purgeobl e Aromot i cs
IEfl Semple No. 350019 4
Sample Identification /;rea ! -Bottom ,.
Date flnelyzed September· 12, 1988 By Co rn'.•ie 11
Results
N•Jrnber Com00untj Duanli\a\ion Li rnil Con(:entration
u.q/f::.1 uo/r'.o
Benzene 1 (·1 ..... , BQL
,; Ch l orobenzene 1.0 B!JL L.
7 1 .2-Di ch l orot,enzene 1.0 BC!L
4 1,3-Di c1·1 l orobenzene 1.0 BQL
5 1,4-Di cl11 orobenzene 1.0 BOL
6 E t.h1dl t,enzene 1.0 BQL
7 Toluene 1.0 ti I '
8 ~:ul enes 1.0 81JL ··'
"
• FIELD SA,'(PLI,:G-UffORi'LI\TlON SHEET
CHAr~, o, CUSTODY REcoA
(Hazardous ~!aterials and O~rs)
1:01~: This £0r.n ::iust be completed prior· to processing samples in Laooratoc,. c:o
5a~ples will be processed without Job ~lo. ~nd Dilling. Inscructio~s.)
Job '.lo . : __ ..cP-c·c.......cOc...e-.:N.:.:oc...,__4.:.:0c..1""5""6"-------Laboratory Sample ~lo.-': ___________ _
(Lab Use Only)
Clio?nt or System Name: Channel Master --~=~~~=~=------------------------
Councy: Johnston ----------------
Address: P.'0. Box 1416
Date Collected: 0 Sc'(J l9S::S
Sa::,ple Location or Description:_~~~~~~~s~o~i]lc.Jf~r~o~m~V~O~C_sc~o~n~t~a~m~1~·n~ae.ttgegd_;ia~r~e~aL ______ _
at the Oxford, NC Cleanup Site.
Type oi Sar.1ple: 0 \.lacer O \4astewater O Sludge O llazardous \.laste [ju Ocher Soil
If Ha:adous: Type Code (if any): ---------DOT or EPA ID tic.: _______ _
Field Infer.nation/Comments (or) Samolc Handling Precautions: ______________ _
I hereby certify that the above information .is correct,
,/; f .. •· ;> •
Collector's Certification: C:(c,.,/\, ·T· /:;-,, ·: --'---'--'-"'--'---"---'-'~'-'---'-~---------------------
/ (Signature)
"Sa;;,ple Allocation" and "Chain of Possession": (Sign & Date in Ink)
D~tc 3ignat:ure ·' ' // / ,, ,
l. Sar.ip le Collector: ,,{_/ / I •, /',JI., . J '•;•
2. Sai;,ple Transporter:
J. Sanple Received in Lab:
(__
4 Sa::iple Ana l.y sis Completed:
Lab Test Reaucsted (List Below): Level I
Method 601/602
Lab Silli~, Instruction: -----------------------------------
'.
• •
Commen\1 BOL -BELOV-l QUi\t-lTITATIDN LIMIT
Purgeable Halocarbons
I EA Sample No. 35001 9
Sample Identification Area 2-Adj. to ,Jit,::h
Date Analyzed September 12, 19t::3
Number
2
7 _,
4
5
6
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
Chloromethane
Bro mo methane
Vi n!Jl Chio ride
Compound
Di i:: h lo rodi t7 1Jo ro rnet_ ha ~1e
CM o r·oet h,; ne
MethtJl~nc chlo:-id(:
T richlorotl uor-omethane
1., 1-Dii::~1loroethB11e
1, 1-Dict1lo1·oeH1ane
tr;3rr::-1 _.2-Didiloroethene
Chloroform
1,2-Dii::hloroethane
1, 1, 1-Tr"ict11oroetJ,ane
C.~rbon tetnschloride
B rnmodichlot·omethane
1,2-Dic!1lon:iprop;rne
tran~;-l _,3-Di(hloropropl:!ne
Tri c ~1lo r·oet r1e ne
ci;,-1,3-Dichloropropene
1, 1,2-Trictiloroethane
U1lorodi br-ornomethane
2-Chloroett11Jlvin1J1 ether
Bromofor·m
T et rac hl oroet ~iene.
1} 1 }2}2-Tet.rad1loroethu1e
Chlorobenzene
1 ,3-Dic:hlorobenzene
1,2-Dichlorobenzene
1 ,4-Dichlornt,e.nzene
By Corm-.'ell
Ouantita\ion Limit
.\lQ.lrg_
1.0
1.0
1.0
1.0
i .0
1.0
1.0
I 0
10
1.0
1.0
1.0
1.0
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1 . C:
\ .0
Results
Co n,::e nt t·a\i on
.\lQ.lrg_
Bi.IL
BQL
8QL
BQL
E:QL
SOL
BOL
BQL
BQL
E:!JL
8QL
BQL
8QL
BOL.
BOL
BQL
80L
1
8QL
BOL
BQL
BQL
BOL
BOL
BQL
E:t:il
BQL
8Ql
SQL
.,
'.,s:: : , . .,. .. -..... " .... ,-r, ;,: , ,
;,,A•
C
• •
Commenb BQL -BELOV-i CIUMITITATIOl·I LIMIT
Purgeoble Aromatics
I EA Sample Ho. 350019
Sample Identification Area. 2-Adj. to ditch
Date Anal •Jzed 3epternber· 12, i 9:3::;
!-!umber· C(1mpound
Benzene
r, Ch 1 orobenzene ,._
-;; 1,2-Di c:1·1 l 01-ot,enzene
4 1,3-Di ch l ornt,enzene
5 1,4-Di ch l ornbenzene
6 rt1·q1t~ .. ,-,·-t l __ 1 lr;:1!"-C-1lt:
7 Toluene '
Q u vql P. .... P .... I',__ -· t I-·-:•
By Corn•.-lell
Results
Ou-ant.itation Limit Co n•::e nt. r-ati on
u.o/Kq u.o/1'.q
10 BCIL
1.0 BOL
1 ,-) .•._.< BQL
1.0 BC!L
1.0 BOL
1.0 BC!L
1.0 C ·-'
10 8QL
• FIELD SA:fPLl>:G UIFOWl:\T 1011 SIIEET
Cl/A u1 oi: cu:iTOl>Y 1u:c.
(llazardous '.lat~rials .ind Others)
~:OTO::: This r"ur.n ~ust be completed prior to proccs:.ing sJrnpli2s in LaborJtv:-/. c:o
sa:nples will be proces5ccl wichouc Job no. nnd Billing ln$tructions,)
Job :1 o . : ___ P:..· .:..· _·.=O..:.._,_N""o'-'.'---'1'-', Oe...1~5,,_G"--------L.,.bor.,tory Snmplc ~lo.~=------------
(L1b Use· Only)
Client or System Name: Channel Master __ _;==='-'===-------------------------
County: ----------------Johnston
Address : ___ _;P__;•c..'_;Oc.:·c..__;B:.:o'-'x"-'l'-'4'-l'-'6"---------------------------------
(' Date Collected: -,c:. i )'(, Time Collected: (:1cs.) ---'--'---------....:...:.:..:....::...:...:... ~"-----'--+---'~-------
Sa np 1 _e Loe a t !. on or Des c rip t ion : -~~~~!!~.:2s.o:0'1iJlc__J[~1i:!co~1!!_n_V':'.'QOfC-'ccs:oc1:n!..!tJa!!nll_;11i_J' ':.!:' ae.l_tgcgcl_iJac.!r:.C:eccaL ______ _
at the Oxford, NC Clcnnu Site.
lf Ha:ardous: Type Code (if any): ---------DOT or EPA ID tlo. : ________ _
Fielq Infer.nation/Comments (or) Samole Handling Precautions: ---------------
I hereby Certify that the above infoCT11ation is correct,
C 11 ' C ' f' ' ;,.) I ,·. . . . o _ector s ~rt1 1cat1on: __ ...1....~1__,_r~,-~,c..·__;(~, __ ,_1_._;·_·_·--'•. ____________________ _
1 (Signature)
"Sa"'ple Allocation" and "Chain of Possession": (Sign & Date in Ink)
., . Signature Date
1. Sanple Collector:_....,__i~/~1:~,--(~.,~:,~~-~---t~_-'-/_;_;_.-_,._c_i_,~'·----------1-~I~-·-·_.~-•-··_/_/-+-'!-'-;~,~;-· ___ _
2.
J.
Sa.r.1ple
Sanp le
Sa::iple
Transporter:
Received in -La_b_:_d-,~_ ,~)-o~-~-j-_~J~~-__ \.,:_Q__t~;l-(~-n_-.~-"-~Q~. ----~L-7---2--j}-. ~i--,-2-_-;-uc)_l __
Analysis Completed:
1 I -------------------'-------'--------
Lab Test Reauested (List Below): Level I
Method 601/602
_Lab Silli~5 Instruction: __________________________________ _
· .. ·i----FORMOFPAYMENT ·• ·.1 -@!il!fil@lwf!il I UNITED STATES I CANADA 11 INTERNATIONAL I '.
STANDARD SERVICES ,. STANDARD SERVICES •
cAsH □GaL □ r FCCOD □ WDRu:MRDIE Samo Day □ Othor □ , Couriar Express □ Bvsinass □ Documents , CBL
Next Morning ~ Metro □ Air Cargo S•ryice D Customs □
D 1 8 D 3 5 5 7 7 T Clearance
· PPD fg. COL OoTHOcoMAr □ S8CO/Jd Morning O : □ 'Air EConcmy Sarvlca D Dal/very □
i:l cf 'ff[f{;'S"'ltf ~tJ . l lllll lllll lll!I IIIII II Ill II Ill II Ill lllll lllll lllll lllll llll! 9-a::Sa I ii5u I :cr:1_8]0":fs1s~:;r(]
From: To: Tariff Desi. '.I Gatew~~i --~
(919) 733;..2so1 Saturday
. ·Roger Coato [phone] Jach: BuJilalr Dal/very D
CHANNEL MASTER -C. 1$ I ' UC Dope of BUii!!lD lloOOUlt'COO CERCLA 0,
0. . Hold □ 1-100 -. JNOUSTRIAL PARK ·DR 306 n; Wiloington Stli:cot • ., □ □ 10(-300 ' , Airport I Cmd, ~. Canada □ □ 301-700 ·0
·~ SMITHFIELD, NC Rlllotgh .NC n □ 701-300w -. □ · Customer's Reference Numbers · Zip E Consignoe's Emery Accou?.t No. Zip 3001-~0l , , ,· .~ , 27577 .27601 □ 8001-:Over
9scf/p/1on an ~· Dim9nsi011s P19C9S • ' r .. .. ' w H (In Lb$.) ' ' "Lab Results □ ,·j
. ~ ,
· .' roDSRO HazMatO . £di;□ .. 0[!)@[£)[!]0[£1 1 I 2 I 3 4 I 5 I s 2 ? ,o G · 1 I a I e 0 1 I 2
,
I
uJ I
··-:· ·.-,;:p··(i.·..1-1 Ql Pac*
son,ck
,, .. .,,., ~
0 ~-12X15 :< Terms and Conditio Shipper's Sinnature X rP'v"li •· 00~ \.,i) I,<){__ I , ,
n/9ma/lOna ,£"'9s '' Third party bilfiniJ , a , l=m9~ Account Ne.
Comm. Code• · only accepted Mc. J,n feb Ma, Ap, M,y ,!un Joi A11g sdP. Ocl No, o,c Multiple Shpts. I Drop Box ' p,., □ l with Emery , E o,y 1 ;2. ,3 4 ·s ,,,e:, ,7 ·a· ,,9 ·:o • 1 2 ·1 2 3 I 4 · 5 I s Domicl/o · Account No. Time .. . Intl. Cusroms Vafuo I · Intl. lnsi.Jrance Rec"d " 1 0 1 2· 0 2· 1 •'":.: oo· :,,.· 15 ·,.7 ·B; s ·1 o_• -1. 1· 2 -At Origin By Hour ....... .. , 1--'--Emory Time 3 4 5 8 7 8 9 .30, 45 -. . '"" ,,, Ovor . · , ,
~as8 Chafge · ' cw,er ' Sl11PIWJ [3 [),op □ 01 By: Emory R'fP,BS(!ntative. "Y. Total Transportation Charges □ I OC-
Good, Al Destination Roc"d •= -.. t· !.7-'. $ At: Em•ry .rl.C•"'" ri fil ' ,, i• ' , ..... TOTAL T,rmmal c•
,-! .. ·.--.-x .... , .. , '. ··-·
.• 1.,
. ,
i.
• •
Comments BQL -BELOW QUAIHITATION LIMIT
Purgeflb1 e Ha 1 ocorbons
IEA Sample lfo. 350019 §_
' Sample Identification Area 2-Adi. \•J Drqer
Date l'lne1 ~zed September· 12 1988 B•J Curr•J
Numt>er
2
7 ._,
4
5
6
7
3
9
10
11
12
13
14
15
16
17
18
19
20
21
24
,:, C' ~"
26
27
28
Ct, Io ro methane
Bromometh,ine
Vinyl Chloride
Compound
Di::: h io rodi fl uo ro rnet ti;:1 ne
ChloroBth;;;ne
f-··lethiJlene chloride
Tr·ichlorotl uoromethane
I, 1 -Dict·,1oroe\hene
1, 1-Dichloroethane
trans-1 .2-Dichlornethene
Chloroform
1,2-Dict,loroe!hane
1, 1, 1-Trict,loroetr,ane
C3r·bon telrechloride
E, rn mo die h 1 o 1·0 methane
1,2-Din,loropr·opane
t.r,rns-1,3-Dichlot·opropene
Tri c hlo roet he ne
r::i::;-1,3-Dichlc.ropropene
1, 1,2-Tt-ichlot·oeth:;r,e
Chlorodi bromometk1rre
2-Ch1oroelh9lvi n,,1 ether·
Bromoforrn
Tetra,; hi o roet he ne
1, 1,2.,2-Tetr~(=hloroethene
Chlorobenzerre
1,3-Dichlorobenzene
1,2-Dlchlorobenzene
1 ,4-Di,)ilor1Jbr,m:ene
Ouantitation Limit
Llq / f~q
1.0
1.0
10
1.0
1 0
1.0
1.0
1.0
1.0
1.0
1.D
1.0
1.0
1.0
1.0
1.0
1.D
1.0
l.O
1.0
1.0
1.0
1.0
1.0
1.0
LO
1.0
1.0
1.0
Results
Co n,;e nt ration
uq/f'.q
BQL
BQL
BQL
BQL
BOL
BQL
BQL
BQL
BQL
EiQL
BQL
BQL
BOL
BQL
BQL
E;QL
BQL
BQL
BQL
BQL
BOL
BQL
BQL
E;QL
BQL
BQL
BQL
BQL
!lOL
...... , -
• •
Comrnent3 BQL -8ELOV1 QUi;NTIT,',TIOl·I L!l11T
Purgeoble Aromatics
I El\ Sample No. 350019 .§_
Sample identification /\re~ 2-Adj lo D1·qer
Date f\nalyzed 3epternbn 12, 19:3::; By Cuny
Mumber
2
4
5
6
7
6
Compound
Benzene
Cl1 l ornbenzene
1 ,2-Di ct1 l 01·obenzene
1,3-[li ct·; l ornt,enzene
1,4-Dichlon:,benzene
Eth,pbenzene
Toluene
Ouentitl:!tlon Limit
1.0
1.0
1.0
1.0
1n
1n
1.0
1.0
Results
Con•~~ntretion
ll.'l /Kg
BQL
BCIL
BIJL
BOL
BQL
2
•
FIELD S,'--''(PLI,:C UfFORl-l".TlO{!HEET
· , CHAI:! OF CUSTODY REC
(Hazardous ~1.:iterials and Ot 1crs)
~:OTE: !his f,,r.n ·•1•Jst ~c comr,lcccd pri.Jr to rrocc~:oing ~nmplt!5 in Laboraco~i'• (~:o
s&~pJes uill be ?recessed wi~hout Job ~lo. ~r1tl Billing Instructions.)
Job '.lo.: P. O. Nn. l1015(, L.1hor,,cory S;,mple ~lo.: ---------.,---(Lab Use Only)
Clil:?nt or System Name: Channel Mnstcr --....:::==='---'===-----------------"--------
Count)': ---------------------Johnston
Address: P.'O. Box 1416
Dace Collected: lP Se J { <'( <;;'( Time Collected: //(i0 (:i~s. ---------------
Senple Location or Description:_~~~~~!._~s~o~·:Jl:_Jf~r~o~m:ii._VY.QOIC___sc~o~n~t~a~m~i~1~1a!U_tgcQ<l__i!aUr~e~aL_ ______ _
at the Oxford NC Cleanu Site.
Type oi. Sar.ipli?: 0 Water O Waste...,•atcr O Sludcc O llaz.a."rdous W.1ste [KJ Ocher SoiJ
If Ha:ardous: Type Cede (if any): Derr or EPA ID 110.: --------
Field In for.nation/Comments (or) ~le Handlin&_ Precautions: ______________ _
I hereby certify ch.1c the above information is correct,
Col!ector's Certification:_...,,_10~t~c_._~~/!_,~,s~/-~~~--~/'--'-,~-'~;~,:~,._·,~\---,------------------
7 (Signature)
"Sa:::ple Allocation" and "Chain of Pc,ssession":
'
I. Sar.iple tkL, Collector:
2. Sar.ip12
~ (
Transporter:
J. s~r:ip le Rec~ived in Lab:
~. Sa:aple Analysis Completed:
Lab Test Reau~sced (List Bclo1J): Level I
Method 601/602
Lab Silling Instruction:
(Sign & Date in Ink)
Date
I ,r·
------·-----------------------------
Sped al
)l,,f:t1-( C
0
Ins-ruci:ions or
cl:lr,~-CLI<·'{
V
,, . .,..
..
• •
Comment, BQL -BELOW Ql_li\NTITATION LIMIT
Telrachloroeth1Jlene and 1, 1,2,2-Tetrechlor-odhane coelute. GC/l'IS
an;3J 1J:::is i:3 recommended fot· e:onfi rrn;:ition.
Purgeoble Holocorbons
I EA Sample No. 350019 7
Sample ldentificetfon /\t"e,; 2-Adi. to build.
Dato l'lnol gzed ::;eptw,ber 13, 1 98:::
Number
r,
L
7 •'
4
C ·-'
6
7
ci
9
1 I)
1 ' ' 12
13
14
15
16
17
1 0 ')
19
20
21
.-,.-, LL
?< -~
24
,, C" L•'
26
27
28
29
Chloromethar,e
8 ro mo methane
Vi n1Jl Chloride
Compo11nd
Di c hl o rodi tl uoro met h~ ne
Chlor·oen,ene
Meth,Jlene chloride
Tt"ict,lorntl uorometha ne
! , 1-Dichloroethene
1, 1-Dichloroeth,rne
\ran$-1,2-Dichloroethene
Chloroform
1 _,2-Dichloroet.h:1ne
1, 1, 1-Tl"ichlo1·oethane
Carbon tetrachlo•·ide
Bro modi ch 1 o 1·0 methane
1 _,2-Dictiloroprop:rne
tr,,ns-1,3-Dichlorc•propene
Trichloroethene
ci~-1,3-[,ichloropn,pene
1, 1,2-Tl"ichloroeth,3r,e
Ch1orodi br-omornethane
2-C hloroeltilJ lvi n1Jl ether
Bromofonn
Tet ,·,ic t, loroet he ne
1} 11 2.,2-Tett-achloroethene
Chlo ro t,e nze ne
113-Dichlorobenzene
1,2-0i(hlorobenzene
1,4-Di,;hlo1·ot1en.:ene
OuantiMion Limit.
u.q/f'.q
1 0
1.0
i .0
1.0
1.0
1.0
1.0
1.D
1 0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
i.O
1.0
1.0
1.:J
1.!J
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Results
Cori•~':! nt ration
uqn~q
EQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
E:QL
BQL
BQL
BQL
BQL
::QL
BOL
6QL
BOL
BQL
BQL
BQL
BOL
BQL
BQL
7
BQL
E:Cil
BQL
E:QL
BQL
,. ~~:·: . ·'.
. . '
-,, ..
,. ,_.·~~-..
'·; I~ --
• •
Comments BQ L -8 E LO\·'/ (I UA NT lT AT ION Ll II IT
Purge!lbl e Arom!lti cs
IE/\ Semple No. 350019 l
Sample Identification Area 2-Adj. to build.
Date l\nallJzed September 13. 1988
Number· Compound
Benzene
.. -) c1·,1 orot,enzene "-
3 1,2-Di cl1 l ornbenzene
4 1,3-Di ch I orobenzene
5 I _,4-Di cl1 I ornbenzene
6 EU11Jlbenzene
7 Toluene '
~ 0 Vwl ope,,-. (', ._ I._. I'-·.:,
By E:aileq
Results
Ouantitation Limit. Concentration
ua/1'.q ll.·J/1'.q
1.0 B!JL
10 Bl)L
1.0 BOL
1.0 BOL
1.0 BOL
1.0 c-L ul.1
10 r, L
1.0 EiiJL
•
FIELD SA.c'!PL nc l}ffOR!-lf\ TION ~ET
· CllJ\1:1 Or CUSTODY RECOR.
(Hazardous Materials and Otl1ers)
~:OTE: This for.n :Tlust be completed prior to processing samples in labor3ta~/. c:o
sa~ples will be processed wichouc Job No. nr1d !]illing Instructions.)
Joi:, '.Io . : ___ P....:.. . .....c.O.c.. _N.cn--0._l'--1 0'--1'-'~'-' r,"-, ______ _ L,boratory S.,mple No.: ------------(Lab Use Only)
CU.ant or System Name: Channel Master -----'-==='--'===-------------------------
Johnston
Address: P. ··o. Box 1416
Date Collected: '/;? .)c-f" /f[;f Time Collected: __ ~/'--/_(_!_(_1 ______ '--(~_7,--S-'-.)'--
Sa~ple Location or Description:_~~!'!!!!!!"!!'!~~•~ojijlc.Jfjr~o~m~V~OQ.£C__scgo~nUt~n~m~i~1~1aitte~d!L~a~r~e~aL_ ____ ~--
at the Oxford, NC Cleanup Site.
Type o[ Sar:iplt?: D Water O Wast<!woter O SluclF;c O lla.za."rdous Waste fiJ Other Soil
If Hacadous: Type Code (if any): ---------oar or EPA ID tlo.: ---------
Field Information/Comments (or) Samnle Handling Precautions: ---------------
I hereby certify that the above information ip correct, 1/ I/ //
Collector's Certification: J_J.,_J~·r/ f(·ei!.:::r·
----'--'---'--'--'-7r----'---'(,-S,--1-• C-' -11-,1-t_l_l r-e-,--) ------------------
11Sa.:7,ple Allocation" and "Chain of Possession": (Sign & Date in Ink)
,,
I. Sar:iple Collector:
,,; '.) . I l (I. _( ( /
D~ce T~~e (~~s.)
fr-.(i'i,, 1. .f /: "r'T)
2. Sample I Transporter:
J. Sar.iple Received in Lab: (l_,'M.)
~. Sa.C1ple Analysis Completed:
Lab Test Reauested (List Belo1J): Level I
Nethod 601/602
Lab 51lli~g Instruction: -----------------------------------
. ,_ _.
.,
-· '.
• ;'
1
1ti . ">~ ' -~ ... . < .. '".""; ---
'. . { :•.-,,· :;:; ' . -"
-'
' .
• •
Comment. BQL -BELO'•N QUMITITATIOM LIMIT
Purgeeble Helocerbons
I Ell Sample Ho. 350019
Sample Identification At-ea 2-8ottorn
Date Analyzed Septem~er 13, 198:::
t,l!Jir-j~,er CornDoJJnd
Chlo r·ornetha ne
2 Bromometti;~ne
3 Vinyl Chloride
4 Die t,1 o ro,Ji l7 uo 1·ornet hane
C Chloroett,ane _,
6 Me\h1;le11e ct,loride
7 T richioro!l uoromethane
i:i I, I-Dict,loroethene
9 I, I -Dichloroethane
10 trans-l .• 2-[Ji c 111 o n:r~t he ne
11 Chlorofor;n
12 1.,2-Dict,loroeth::ine
13 1, 1, 1 -Tri,::hloroettm,e
14 Carbon tetr;:ichloride
15 8romodich1 oromethane
16 i ,2-Dichlon)prop;3ne
17 \1·ans-1,3-Dichloropropene
' ,-, T I·ichl o roe\ he ne 10
19 ci,,-1,3-Dichloropropene
20 1, 1,2-Trichloroethane
21 Chion:idi btorn(rrneth:Jne ~-, L~ 2-ChloroethiJlvi n1Jl ether
.-}-:: 8l'Omoform .::..J
24 Tel ra,:: ,,1 o I·oet t,e ne
-·:, C" '-·-' 1, 1,2,2-Tett-achk•roethane
26 Chlornbenzerre
27 1,3-Dichlor·obenzen~
2::; 1 }2-Dic:hlor·obenzene
29 I ,4-L1ict1l1Jr,ibenzene
By Cun·q
Results
Quantitation Li mil Concentration
uq/Kq !l1ili
i.O BOL
1.0 BtJL
1.0 BQL
1.1) E:QL
1 0 BQL
1.0 BQL
1 0 BOL
1.0 BQL
1.0 BQL
1.0 BQL
1.0 BQL
1.0 BQL
i .0 BQL
1.0 Bi.IL
1.0 BQL
1.0 BQL
1.0 BQL
1.0 9
i 0 BQL
1.0 BQL
1.0 BQL
j .0 80L
I 0 BOL
1.0 BQL
1.0 BQL
! .0 BQL
1.0 BOL
1.0 E:QL
1.0 8QL
• ,(r• •
,..,_.,., J :· .. _ .....
. ;,_ ... ·.
-~, .:'•, .
... . ..:.:,. -
• •
Comments BQL -BELO\'/ QUANTITATIOl·I LIMIT
Purgenb 1 e Aromnt i cs
IEl'I Sample Ho. 350019 §_
Sample Identification Area 2-Boftom
Date Anel!Jzcd SeDtember 13 1988
Number Comoound
Benzene
2 Ct'1lornbenzene
3 1 ,2-Di ci·, 1 orot,enzene
4 1 7 -r,;0·t·1 -t-·,-·-,·-' ~·, '-· 1 Ol O lt:tl~t:llt:
C: ~' 1,4-Di ct1 l ornt,enzene
6 EtJnd1 t,enzene
7 Toluene '
B y;,~1 enes
By Currq
Results
Ouantit,tion Li rnit CorP::~ntrl':!tion
u.,1/l'.a .u.q/k:g
1.0 BQL
10 BQL
1.0 BQL
1.0 BDL
1.0 BC!L
1.0 E,QL
10 BlJL
1.0 EiQL
•
FIELD S,~'IT'Ll::G UIFOIU·IATIO.t-1 SHEET
CllJ\1:1 o,-CUSTODY l(EC
(llazardous ~acerials and Otl1ers)
~:oT::: This Cur.n ~ust be comi,lctcd rrior to proccs;, i.np, s,,mpl~s in LJbor.JtO:-j'. (;:o
::,a:nples will be Processed without Job no. ,,nd Hilling In!":r.ruction~.)
JO b '.lo. '---'P'-'-. -"-o_. ---'-N~o~·-'•~O~1~5~6~------Labor.,cory S,,mple ~lo.: -----------(Lab Use Only)
Cli~nt or System N~'l.me: Ch.'lnnel Mnstcr -------~~~------------------------
County: Johnston ---------------------
Address: P. · O. nox l/,16 -----=---'-="-'c.c,_=---------------------------------
T i me Collected: ---'---------------
5 an pl e Location or Dcscription:~-~~~~~~~s~o~iJ.l~.Jf~r~.0~1~11_V~O~.~C.....5:c~o~n~tin~n~ii~1~1.1ll_tc£.Qcl__B.1ir~e~aL_ _____ _
at the Oxford NC Cleanu, Site.
Type· oi. Sar:'!plt?: 0 Water O Wastewn.tcr O Sludcc O llnznrdous W.,ste (xJ Ocher Soi
If Haeardous: Type Code (if any): ---------Dar or El'i\ ID tlo.: --------
Field Inf or.nae ion/Comments (or) Samo le Hand 1 ing_ Precautions: _____________ _
I hereby certify that the abov~./nf?rmati,rnj~ correct.
( 0 l le C t Or ' S ( e rt i f i C ,1 t i Oil : __ Au·_.,.(ce, C-c.j'-';lc,,Je-' --''.'-· _· _,_;-''._,·._,_,. ·-''-1-'I, ---------------------
/ (SJ.gnaturc)
"Sa.::ple Allocation" and "Chain of Possession": (SiGn & Date in Ink)
1. Saraple
2. Sar:iple
J. Sar.iple
4. Sa..-,ple
1) ;J
Collector: /Ccl.l!~(.:, ~·§.<i._jr.( (,·, f'\:s· 5·C)
__ _,_,_'-"--'-'-'--,7"---'---'-'----'--'--"=---''-'--------P----'---t---'---'--"-'---
T rans port c r:
Received in -La_b_: __ /"':1;_v_VlJ--;/J_•r-J<J"1-,--l-tJ2-s.-cc-,,-,,:j_-;--;------i-L--c}-J-t-~-J1-. ,i-/-2--U-'L)-,--
Ana l.y sis Completed'------------------'------'\ _____ _
Signature
Lab Test Rcavested (List Below): Level T.
Method 601/602
Lab 51lci~5 Instruction: -----------------------------------
Sper!al Inscr\l't'on°. or C=1mnn•0 ,· 3 I /)1,,-·/ ;'() fi'.°, j-i,_f-\
• • • ' ., ~" • "" _..;::..-_. c:.1:c.11Ly·-'-T_.11'-'r.,.r1"11,.r,.,Q,.1 .. ,n .. ,:,;.1 ____ ....... ,· ....... ,_ .. _______ , ______ _
•
North Carolina Department of Human Resources
Division of Health Services
P.O. Box 2091 • Raleigh, North Carolina 27602-2091
James G. Martin, Governor
David T. Flaherty, Secretary October 12, 1988 Ronald H. Levine, M.D., M.P.H.
Dr, Mark Mcclanahan
Agency for Toxic Substances and Disease Registry
Building 30-S Chamblee
1600 Clifton Road, N.E.
Atlanta, Georgia 30333
Dear Dr. Mcclanahan:
RE: Channel Master NCD122263825
Industrial Drive
Oxford, NC 27565
State Health Director
Enclosed please find the letter and laboratory data
submitted to our office by Mr. Roger Coats, Channel Master, on
October 5, 1988, as we discussed in our telephone conversation on
~ctober 12, 1988.
You will note that this data indicates maximum levels of
soil contamination in the bottom of the excavated area to be 46
ppm cis-1,2 Dichloropropene. As we discussed in our telephone
conversation on this date, the excavation of soil is down to the
water table. Ground water contamination with halogenated
hydrocarbons has been documented on this site and will be
addressed in future activity. The soil excavated from this area
has been "processed" by passing it through a rotary dryer on
site. The maximum contamination in this processed soil is 68 ppb
2-Chloroethylvinyl ether, 20 ppb Methylene chloride, and 16 ppb
Trichlorofluoromethane. Channel Master desires to use this
"processed" soil and off-site fill dirt to refill the excavated
area.
Your comments on this data and planned filling of the
excavated area are appreciated. If you have any questions or
need additional information, please contact me at [phone].
JB/ds/ibm.28
Sincerely,
Jack Butler, Environmental Engineer
Superfund Branch
Solid Waste Management Section
TO:
FROM:
RE:
• •
12 October 1988
File
Jack Butler
Telephone conversation with Dr. Mark A. Mcclanahan,
ATSDR, (404-488-4100), about Channel Master,
NCD122263825
Dr, Mcclanahan was contacted on this date to discuss the
halogenated hydrocarbon remediation at the subject site and Mr.
Roger Coats letter of October 5, 1988. Dr. Mcclanahan was
informed of the excavation near the loading dock and that
sampling indicated maximum levels of 46 ppb cis-1,3
Dichlorepropene at the bottom of the excavated area. This
excavation is presently at the water table and ground water
contamination has been documented on this site. The soil
excavated from this area has been "processed by passing it
through a rotary dryer on site. Channel Master desires to use
this ''processed'' soil and off-site fill dirt to refill the
excavated area.
Dr. Mcclanahan agreed to respond in writing if I would
submit the data from Mr. Roger Coats letter of October 5, 1988.
This package should be mailed to the following address:
Dr. Mark Mcclanahan
Agency for Toxic Substances and Disease Registry
Bldg. 30-S Chamblee
1600 Clifton Rd., N.E.
Atlanta, GA 30333
JB/ds/ibm.28
I•.,
December 21, 1987
Ms. Barbara Hansen Benoy
Environmental Scientist
U.S.E.P.A.
Reg ion ry
Superfuhd Branch
Site Management Unit NC/SC
Groundf\Floor
345 Courtland St. N.E.
Atlanta, GA 30365
Dear Ms. Benoy:
.: I••;.
As noted in our phone conversation on December 18, 1987, review
of our files by our legal representatives revealed that EPA Form
8900-1 Notification of Hazardous Waste Site had not been
submitted. Therefore, the attached completed EPA Form 8900-1 is
~eing submitted to update our file.
If you have any questions or need additional information
concerning this matter, you may contact me at [phone].
Sincerely,
Roger Coats
Saf~ty & Environmental Engineer
RC/dw
cc: Charles Hansen
Dixie Laswell
Joe Friedman
Jack Butler
I >I" : f ~. r '1 ('
A
l\lot1t1cat-ot Hazaraous vvast-te Environmental Prolect1011
Ag1incy
Wash1noton DC 20460
This initial notification information is
required by Section 103(c) of tt1e Compre-
hensive Environmental Response, Campen•
sarion, and Liability Act of 1980 and must
be mailed by June 9, 1981.
Person Required to Notify:
Enter the name and address of the person
or organization required to notify
Please type or print 111 ink. lf you neecJ
additional space, use sep.1rate sheets of
paper. Indicate the letter of the itcrn
which applies.
~N~'"cc'•~_C_h_a_n_n e 1 Mast e r , ~_i~ i__:i_~_o n o_! __ A v'_ri~ -~ I _n_c_. ____ _
Street Industrial Park Drive
---...... ------. ---·----------------------------------
Smithfield NC 27577
Ccc'cc'Y~--~ ------· ____________ 5~~.!_t;__ ·----·---Zip Co_dc ___________ _
B Site Locati!_m: Narneo!S.n.~e_C_hannel Master, Division of Avnet, Inc.
Enter the common name (if known) and
actual location of the site.
---------··------------
s""' __ .. )_n.<:l U_§..t ~ y_p r. i_'!_~---------. ------------
Ci1v Oxford Cour11vGranvilles1ate NC
C Person to Contact:
Enter the name, title (if applicable), and
business telephone number of the person
to contact regarding information
submitted on this form.
Narne(Last Firsta11dT1tle) Coat::: f Page!:" f Safety/Env • Engineer
--· ----·-·--··-· -··--·-··--·--··-··----· ··-----· --------·-·-· ... -· . -----
Phone ( 91 9 ) 9 3 4 -9 711
D Dates of Waste Handling:
Enter the years that you estimate waste
treatment, storage, or disposal began and
ended at the site.
From (Yea_n __ l_9_6 S
E Waste Type: Choose the option you prefer to complete
Option I: Select general waste types and source categories. If
you do not know the general waste types or sources. you are
encouraged to describe the site in Item I-Description of Site.
General Type of Waste:
Place an X in the appropriate
boxes. The categories listed
overlap. Check each applicable
category.
1. rn Organics
2. □ inorganics
3. D Solvents
4. D Pesticides
5. 111 Heavy metals
6. 0 Acids
7. D Bases
8. □ PCBs
9. D Mixed Municipal Waste
10. O Unknown
11. O Other (Specify)
]·,,rm :\ppr,,vL•d
{),\lB NH. ~000-01,l!'i
FPA f'orm A!lOO·l
Source of Waste:
Place an X in the appropriate
boxes.
1 . D Mining
2. D Cori:;truction
3. □ Textiles
4. □ Fertilizer
5. □ Paper /Printing
6. □ Leather Tanning
7. □ Iron/Steel Foundry
8. □ Chemical. General
9. ~ Plating/Polishing
10. □ Military/ Ammunition
11. o~ Electrical Conductors
12. □ Transf.ormers
13. □ Utility Companies
14. □ Sanitary/Refuse
15. □ Photofinish
16. □ Lab/Hospital
17. 0 Unknown
18. 0 Other (Specify)
To (Year) 1979
Option 2: This option is available to persons familiar with the
Resource Conservation and Recovery Act (RCRA) Section 3001
regulations (40 CFR Part 261).
Specific Type of Waste:
EPA has assigned a four-digit number to each hazardous waste
listed in the regulations under Section 3001 of RCRA. Enter the
appropriate four-digit number in the boxes provided. A copy of
the list of hazardous wastes and codes can be obtained by
contacting the EPA Region serving the State in which the site is
located.
F006
F019 E----=3
I I
i f-----·------~
----
--
-~ ----
i------·-----·-
'----·---
F Waste Quantity: ~
Pince .1n X in tl1e appropriutc bo~
indicate the facility tyµes found at the site.
Facility Type Total Facility Waste Amount
In the "total facility waste c.1moun1" space
give tt1e estimated cornbini~(l quantity
(volume) of hazardous wastes .:it the site
using cubic feet or gallons.
In the "total facility area" space, give the
estimated area size which the facilities
occupy using square feet or acres.
I.
2
3
4
5.
6.
7.
8.
9.
[] Piles
0 Land Tre;itment
I] Landfill
I] Tanks
l!J lmpoundmcnt
D Underground Injection
□ Drums, Above Ground
□ Drums, Below Ground
□ Other (Specify\
"·'"""' so o , o o o_~ o 1 , o o o ,_C!_Q. Q
Total Facility Area
G Known, Suspected or Likely Releases to the Environment:
Place an X ill the appropriate boxes to indicate any known, suspected, XJ Known D Suspected D Likely . D None
attached cleanup plan or lik~ly releases of wastes to the environment. Note: See copy of
Note: ·Items Hand I are optional. Completing these items will assist EPA and State and local governments in locating and assessing
hazardous waste sftes. Although completing the items is not required, you are encouraged to do so. ·
H Sketch Map of Site Location: (Optional)
Sketch a map showing streets, highways,
routes or other prominent landmarks near
the site. Place an X on the rnap to indicate
the site location. Draw an arrow showing
· the direction north. You may substitute a
publishing map showing the site location.
Description of Site: (Optional)
Describe the history and present
conditions of the site. Give directions to
the site and describe any nearby wells,
springs, lakes, or housing. Include such
information as how waste was disposed
and where the waste came from. Provide
any other information or comments which
may help de'scribe the site conditions.
Cleanup of the site is
presently in progress with
the N.C. CERCLA Units
assistance.
J Signature and Title:
See copy of attached cleanup plan
See copy of attached cleanup plan
This plan has been submitted to the following
1. Mr, Russell Wright, Chief
Remedial Action Section
2.
Emergency and Remedial Response Branch
EPA, Region IV
Mr. Jack Butler
N,C. Dept. of Human Resources
Division of Health Services
CERCLA Unit
The person or authorized representative
(such as plant managers, superintendents,
trustees or attorneys) of persons required
to notify must sign the form and provide ;i
mailing address (if different th.in address
1n item A). For other persons providing
notification. the signature is optional
Check the boxes which best describe 1hc
relationship to the site of the person
required to notify .. If you are not required
to notifv cht~r.k "Ottwr"
".".'":cChanneL.11as.t.e.r...,-1liv.i.s.i.on___o.LAvne.t.,_ p Owner, Present
Owner, Past
Transporter
Industrial Park
Su,•1•1
Smithfield C,tv
Drive
NC l,p Cnd1~
27577
□
□
□ Operator, Present
·-fl Operator. Past
Cl Other
..
Dc°par-.mcr,"t ClH:.·~un Resources
-PLE ANALYSES REQ~
State Laboratory of Publi~ Health
ion of He.1ith ~ccs P. 0. Box 28047
306 N. Wilmington Street
.5 '7 Raleigh, 27611
'lumber _,z-'{;-;,; t[) / 7. 7-:Z. C J cf' :z..) Field Sample Number J6'9/
CA a,:,,ue./ ,/La f :f e,-✓ --· .
···s;. Loca:i c:::Jx--ro.,-.c/ /l,/,-C-. .,,
e of.Site .. ate on .-, ,,
.;r, ,:R, dlu"f /e-r ';I-~ e ,.,-j--, / C Io/ ,..P-7 .,
Time /O_iO .
:ctcd By IDII Dat-,.., .
y..t.i. r:.' v £0 /
: of Sample:
,vif'onmcntal Concentrate omments
,'~/, ,, .C-:-/1 __ Groundwater (1) SoUd (5) ea..,.
N 1.!1t.1,.; .11. -,: 1987 :,:: ' -
__ Surface Water (2) Liquid (6) ;i:: S>
~ Soil (3) Sludge (7) ~ /f'<l:'"n!',. ,, ,. ~~
~ ---~~"I w
_ Other (4) Other (8) {)-,... ,.t\~-~w
INORGANIC CHEMISTRY
Extractablcs Total
Parameter Results mg/1 Parameter Results mg/1 Parameter Results mg/1
_Arsenic __ Arsenic __ Silver
_Barium __ Barium __ sulfates
_Cadmium __ Cadmium __ Zinc
_Chromium __ Chloride -,Ph
_Lead __ Chrmnium __ Conductivity
_Mercury __ Copper _TDS
--S~J~f"!iU_!_Tl_ ·-__ Fluoride _TOC
_-Silver __ iron --
-_Lead --
-__ Manganese --
-__ Mercury --
-__ Nitrate --
-__ Selenium --
ORGANIC CHEMISTRY
Parameter Results mg/1 Parameter Rcoulu mg/1 Parameter Rcsulumg/1
&T:GC/MS -EDB __ Methoxychlor
!('Acid:B/N Ext. __ PCB's __ ·Toxaphcne
_TOX __ Petroleum -2,4-D
-__ Endrin --2,4,5-TP (silvex)
-_-undane --
MICROBIOLOGY RADIOCHEMISTR);
Parameter Para.mete_ Results PCV 1
_ (MF) Coliform Colonies/lOOmls __ Gross Alpha
_(MPN) Coliform Colonies/lOOmls __ Gross Beta
---
---
:e Receivt;d 9-/(_p -R7 :;tlHt Date Reported /l--I 'f -J--)
:e Extracted I o --1 · 'il..1 1.1.:9 Date Analy:cd frJ -•z ✓r__ Z ~l~
~ ~µci_.O 70::Z497
oorted By Lab Number
'\./
S JJQj (Revioed 7185)
J 210J Ha:..tirdous Waste-(Review 7/87) .
.... DIVISION OF HEALTH SERV~
..,,D AND HAZARDOUS WASTE MANAG .. BRANCH
Chain of Custody Record
Hazardous Waste Materials
Location of Sampling: Generator __ Transporter __ Treatment Facilit
__ Storage Facility __ Disposal Facility __ Landfill
✓other: C/ec,-t u,JO
Company's NBllle C lzqd-,el /'rQJT er
Address Ox /'o,,,.c,/ /t/4 C-
Collector's Name ~_,,
signature
•
Telephone( 'fl'!) 6 r 3-90 5t c7
Tele_phone( 'rl'f) 7.J.J-..2.8-'0 /
Date Sampled S XV° T, /(;, / o/CJ 7 Time Sampled / t?.) 0
Type of Process Generating Waste.--".<::<;".;~~,e.::::::...fi~a=· ~/--~~~1/a~r....£._,_-~n"-;4';z... __________ _
' /
. Field Information
Field Sample No. J 6 fl
Chain of Possession:
l. @~ 0 · signature .S w:?j; It:: /9' tf,7
inclusive dates
2.
signature inclusive dates
3.
signature title inclusive dates
Results reported
signature title date
Instructions: Complete all applicable information inclucing signatures, and
submit with·~nalysis request forms.
DIVISION OF HEALTE SERVICES
SO~ND HAZARDOUS WASTE l".A.1'AGEMEN~CH
"9 Receipt for Samnles ..
The samples described below were collected in connection with the administration, · enforcement, and documentation of the:
() North Carolina Hazardous Waste Management Rules, 10 NCAC lOF
() North Carolina Solid Waste Management Rules, 10 NCAC lOG
() Comprehensive Environmental Response, Compensation and Liability Act (CERC'J..A)
( ) Toxic Si;bstances C,ontrol Act (TSCA). 15 U.S.C. •s2601, .!:!_ ~-, specifically Section 11 .of TSCJ.., 15 U.S.C. § 2610.
Inspectol'.' s Name
Name of Firm
Finr. 0.."Iler, Ope1·a ~er, or Agent
-
S,'_¾PLE COLLECTED SAMPLE TYPE
KU113ER DATE TD-!E WATER SOIL
·•
I
Receipt for the sample(s) described.
above is hereby ack.c~o~ledged:
Signature of Inspector
Title
OTHER
Inspector's Address
Fim Address
Title
DU?LICATE SA..'iPLES. SAM?LE LOCJ..TION OFFE~iACCEPTED REJECTED oN-sin: Ot:-SITE
. .
i
.-. ~-; -. " ..
I
Receipt/rejection of duplicate or split
sa:c:ples is hereby ackno,.:ledged·:
Signature of Firm Owner, Operator, or Agent
Title
CO~!,TS, ________________________________________ _
-STATE LABORATORY Of PUBLIC HEA,,, DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 21611
ORGANIC CHEMICAL ANALYSIS
BASE/NEUTRAL AND ACID LAB NO '10 ::1u·4--7
EXTRACT ABLES FIELD# :::i;_c; J
COMPOUND TYPE 13 l ( )
UNITS un/Vua/k~ ua/1 ua/kQ
N nitrosodirrethvlamine
bis(2 chloroethvllether
2-chlornnhenol
phenol
l 3-dichlorobenzene
1.4-dichlorobenzene
1.2-dichlorobenzene
bis(2-chloroisnnrnnvJ)ether
hexachloroethane
N-nitroso-di-n~rnnvlamine
nitrobenzene
lsnnhorone
2-n it rnnheno l
2 4-dirrethvlohenol
bis(2--chloroethoxv)rrethane
2 4-dichloroohenol
1.2.4-trichlorobenzene
n>nhthalene
hexachlorobutadiene
4--chloro-m-cresol
hexachlorocvcl~ntadiene
2 4.6-trichloroohenol
2-chloronanhthalene
acenaohthvlene
dirrethvl nhthalate
2 6-dinitrotoluene
acenanhthene
2.4-dinitrnnhenol
2.4-dinitrotoluene
4-nitrnnhenol
fluorene
4-chlornnhenvlohenvlether
diethvl nhthalate
4.6-dinitro-o cresol
diohenvlamine
azobenzene
4-b~henvlohenvlether
hexachlorobenzene
nPntachlornnhenol
ohenanthrene
anthracene
dibutvl nhthalate
fl uoranthene
J -Estimated value.
"??c)
\ I
lb,-V
.=130
/!,,.,O
.-J30
.JI
//_<;?)
-..v
3.~o
=s;., C7
I;_ ,<...-V
33c.7
\.
117DL
~o.C 5011-
(.,{._
I/
K -Actual value is known to be less than value given.
L -Actual value is known to be greater than value given. u -Material was analyzed for but not detected. The nunber
NA -Not analyzed.
1/ -Tentative identification. fl -On NRDC List of Priority Pollutants.
N.C. V-<.v,U.,-<.on 06 He.aLth SeJtv-<.C.e/2
VHS 3068-0 (4/86 Labo~a.to~y)
( )
ua/1 .,n/ka
( l
••n/] ••n/kn
( l ( )
.,n/1 ··"/ka un/ l un/ka
•
BASE/NEUTRAL ANO ACID
EXTRACT ABLES
aJNPOONO
i>vrene
>enzidine
,utvl benzvl ohlhalate
l>enz(a)anthracene
chrvsene
3,3-<lichlorobenzidine
ois(2-,,thvlhexvllnhthalate
di-n-octvl ohthalate
l>enzo(blfluoranthene
l>enzo(klfluoranthene
l>enzo(a)nvrene
indeno( l 2 3-cdlnvrene
dibenzo(a.h)anthracene
benzo(a h. i l=rvlene
aniline
benzoic acid
benzvl alcohol
4-chloroaniline
dibenzofuran
2-rrethvl=nhthalene
2-rrethylphenol
4-<rethvlPhenol
2-nitroaniline
3-ni lroani 1 ine
4-ni troani 1 ine
2.4.5 trichlorophenol
J -Estimated value.
" STATE LABORATORY Of ~UBL!C HEALTH
DIVISION Of HEALTH SERVICES, N.C. OEPARTMENl Of HUMAN RESOOHCES
P.O. BOX 28041 -306 N. WILMINGTON, SI., RALEIGH, N.C. 21611
ORGANIC QjEHICAL ANALYSIS
LAB NO ,,,M,.J <I c;, ''l
FIELD# .:i/-C/ I
TYPE ( 3 l ( l ( ) ( )
UNITS un/ l {\,n/kQ 0 un/ I un/kn .. n/ I .. n/kn un/ l uo/kQ
-=,-_,.o //--
/IA.\?)
.1::, 0
I "./
// ,"2)
.• ''l 0
.·30
lt.,_IT:,
,,,' ' /
I/-.\-V IA..
I
.,j/
.i3o
,,
I b::,<>
' / ' J
tnJlL
,:;,,, 5olL
K -Actual value is known to be less than value given.
( )
un/ J un/ko
-.
L -Actual value is known lo be greater than value given.
U -Material was analyzed for but not detected. The nurroer is the Mini<IUll Detection Limit. ;,1.])L-
HA -Not analyzed.
1/ -Tentative identification.
~I -On NROC List of Priority Pollutants.
N.C. D.i.v.i.J.>.i.on 06 fie.aU/i Sv,.v.i.c.e.J.o
VHS 3068-0 14/86 Labo~ato~y)
( l
.. n/J .. n/ka
•
03 December 1987
TO: File:
FfilM: Jack Butler
RE: Teleph:lne conversation with Roger Coats, [phone], about Channel
Master Site, NCD122263825.
Mr. Costs contacted our office on this date to report the results of
soil sampling conducted on Nov. 20, 1987. The on-site soil sample contained
260 ppm total chromium. Mr. Coats agreed that this material would be
transported to South Carolina as a hazardous waste with other sludge and
contaminated soil from the site. Mr. Coats reported that Channel Master has
begun shipping soil again at a rate of about 20 truck loads per day. They are
also refilling the lagoon with clean fill that was stockpiled on site from the
lagoon area.
Mr. Coats provided the following data for tbe off site soil samples:
Total (ppm) EP Tax
Cadim.trn 0.05 0.02
Chromium 30
Lead 7.75 0.24
Silver 0.25
Barium 2.8
Tois sample is naturally occurri.t1g clay that is intended to be used as
fill material in the lagoon area.
JB/pb/pc
TO:
FROM:
SUBJECT:
• •
November 23, 1987
File
Jack Butler
Telephone conversation with Falecia Barnette, EPA Region IV
(404-347-2234) about Channel Master, NCD122263825
Ms. Barnette contacted our office on this date to inform us that as
part of their HRS package review EPA Headquarters is changing the name of this
site form Channel Master to JFD-Channel Master.
JB/ds/0526b-3
TO:
From:
RE:
•
File
Mary Giguere CIH
Channel Master
20 November 1987
NCD122263825
•
On November 20, 1987 a visit will be made to the Channel Master site by
Jack Butler. The purpose of this visit is to collect samples of fill dirt.
The fill dirt was used to cover the top of an old surface impoundment
and it is being removed so the impoundment can be cleaned up. It is thought
that the dirt is uncontaminated but samples are to be taken to assure that
this is the case.
The Channel Master site has been entered and toured in Level D
Protection. Because of reasons stated in the site safety plan and because the
soil to be sampled is thought to be uncontaminated, Level D protection will be
adequate for this visit. Boots and gloves should be worn while collecting the
soil samples.
• • J. ALLEN ADAMS
WILLIAM H, McCULLOUGH
JOHN 0. BEARD
ADAMS, McCULLOUGH & BEARD
ATTORNEYS AT LAW
E. D. GASKINS, .JR.
ROBERT W. SPEARMAN
HUGH STEVENS
CHARLES C. MEEKER
CATHARINE BIGGS ARROWOOD
WILLIAM G. PAPPAS
ALFRED P CARLTON, .JR
CYNTHIA LEIGH WITTMER
STEPHEN D. LOWRY
F EUGENE HAFER
.JOHN F: GRAYBEAL
LISA M. NIEMAN
BLAIR LEVIN
JOHN J. BUTLER
POPE MCCORKLE, m
GARY S. MAINES
JAMES K. KUYK
HENRY C. CAMPEN, .JR.
ABRAHAM PENN JONES
JILL B. HICKEY
ROBERT W. SAUNDERS
OF COUNSEL
HEMAN R. CLARK
DOUGLAS Q. WICKHAM
Mr. Jack Butler
P. 0. BOX 389
ONE EXCHANGE PLAZA
RALEIGH, NORTH CAROLINA 27602-0389
TELEPHONE [phone]
TELECOPIER (9!9) 834-4564
November 19, 1987
North Carolina Department of Human Resources
Division of Health Services
Solid and Hazardous Waste Management Branch
Post Office Box 2091
Raleigh, North Carolina 27602-2091
RE: Channel Master Site Investigation
Dear Jack:
WASHINGTON, D.C. OFFICE
2000 M STREET, N. W
WASHINGTON, D.C. 20036-3307
[phone]
NEAL A. JACKSON
MARTIN E. FIRESTONE
DAVID P TOWEY
JOSEPH J. LEVIN, JR.
JUSTIN A. THORNTON
WILLIAM LIETH
BARBARA ROWLAND*
OF COUNSEL
SAMUEL H. POOLEt
CARY OFFICE
8000 REGENCY PARKWAY
SUITE 3S0
CARY, NORTH CAROLINA 27Sll-8515
[phone]
CHARLES H, MONTGOMERY
RENE:.E J. MONTGOMERY
TEF<RI TOTH McKEE
0Ml!:Mf!ll!:R CAL,..ORNIA BAJ:! ONLY
lMEMBl!:J:I NORTH CAROLINA eAR ONLY
This letter is to confirm our request for copies of materials that I
marked in reviewing the Solid Waste Division's public records concerning
activities in Granville County. I have marked information concerning
activities by Channel Master and JFD Electronics as well as by nearby
industries. One of the purposes of our investigation is to determine who else
might have contributed to the contamination of the site now owned by Channel
Master, and therefore we need the requested information.
Thank you for your cooperation.
Sincerely,
ADAMS, McCULLOUGH & BEARD
. ' /I
i )~!; ;J,.Y~J
/
John J. Butler
JJB/mho
• •
12 November 1987
To: File
From: Jack Butler
Re: Telephone conversation with Tom Giller, Gessler, Flinn, and Laswell
[phone] about Channel Master, NCD122263825
Mr. Giller contacted our office on this date to obtain information on
the HRS ranking for the Channel Master site in Oxford. He was informed that
our original ranking was forwarded to EPA Region IV for review by them and
Mitre. In late August 1987 this HRS package was forwarded to EPA
Headquarters. Mr. Giller was directed to Felicia Barnette, EPA Region IV,
(404-347-2234), for further information on the ranking for this site.
Mr. Giller recontacted our office later in the day to request a copy of
the PA and SI reports. Mr. Giller was informed that these could be supplied
at a cost if requested in writing.
JB/0520b.23
• • ..J. ALLEN ADAMS
WILLIAM H. MCCULLOUGH
.JOHN Q. BEARD
ADAMS, McCULLOUGH & BEARD
ATTORNEYS AT LAW
E. 0. GASKINS, JR.
ROBERT W. SPEARMAN
HUGH STEVENS
CHARLES C. MEEKER
CATHARINE BIGGS ARROWOOD
WI L..LIAM G. PAPPAS
ALFRED P. CARLTON, JA.
CYNTHIA LEIGH WITTMER
STEPHEN D. LOWRY
F: EUGENE HAFER
JOHN F GRAYBEAL
LISA M. NIEMAN
STEVEN ..J. LEVITAS
BLAIR LEVIN
.JOHN ..J. BUTLER
POPE McCORKLE, m
GARY 5. MAINES
JAMES K. KUYK
HENRY C. CAMPEN, JR.
ABRAHAM PENN .JONES
.JILL B. HICKEY
OF COUNSEL
HEMAN R. CLARK
DOUGLAS Q. WICKHAM
Mr. Jack Butler
P. 0. SOX 389
ONE EXCHANGE PLAZA
RALEIGH, NORTH CAROLINA 27602-0389
TELEPHONE {919) 828-0564
TELECOPIER [phone]
November 12, 1987
North Carolina Department of Human Resources
Division of Health Services
Solid and Hazardous Waste Management Branch
Post Office Box 2091
Raleigh, North Carolina 27602-2091
WASHINGTON, D.C. OFFICE
2000 M STREET, N, W.
WASHINGTON, D,C. 20036
[phone]
NEAL A . .JACKSON
MARTIN E. FIRESTONE
DAVID P TOWEY
.JOSEPH .J. LEVIN, JR.
FORD ROWAN
WILLIAM LIETH
.JILL L. ROWE
OF COUNSEL.
SAMUEL H. POOLE
CARY OFFICE
8000 REGENCY PARKWAY
SUITE 3SO
CARY, NORTH CAROLINA 27511-SSIS
(9191 4-69-1089
CHARLES H. MONTGOMERY
RENEE .J. MONTGOMERY
TERRI TOTH MCKEE
RE: Channel Master NCD 122263825, Industrial Drive, Oxford, N. C.
Dear Jack:
This letter will confirm our conversation of today in which we agreed to
meet on Tuesday to discuss the Channel Master site in Oxford. I would like
to meet with you at 3: 00 p. m. , instead of 2: 00 p. m., as we discussed,
because of a schedule conflict I just discovered. Please call me if 3: 00 p. m.
Tuesday is not convenient for you.
As I mentioned on the phone, our firm is now representing Avnet,
Channel Master's parent corporation, in connection with the CERCLA action at
the Channel Master industrial site in Oxford. In connection with this
representation, we request access to all of your department's files concerning
this site so that we can assess previous activity at the site and identify those
previously involved in activity at the site. While we are interested in looking
at the entire file to ensure the accuracy of our own records, we are most
interested in activity at the site between 1962 and 1979 when the site was
owned and operated by JFD Electronics or affiliates of JFD Electronics before
Channel Master became involved in any activity at the site.
Thank you for your cooperation in this matter.
meeting you.
Sincerely,
I look forward to
ADAMS, McCULLOUGH & BEARD
&~
Jolin J. Butler
JJB/mho
cc: Robert W. Spearman, Esq.
• •
GESSLER, FLYNN, LASWELL, FLEISCHMANN,
HUGHES & SOCOL, LTD.
Mark S. Dym
Thomas J. Fleischmann
Terence E. Flynn
George W. Gess I er
John K. Hughes
Dixie Lee Laswell
Andrew H. PereUis
Donna Kaner Socci
Leon J. Telchner
VIA FEDERAL EXPRESS
Mr. Jack Butler
ATTORNEYS AT LJ>..W
Three First National Plaza
Suite 2300
Chicago, Illinois 60602
[phone]
Telecopier: [phone]
Telex: 728386 HQ LOOP CGO
November 12, 1987
North Carolina Division of Health Services
Solid and Hazardous Waste Management Branch
Environmental Health Section
P. 0. Box 2091
Raleigh, North Carolina 27602
Re: Channel Master Site -Oxford, North Carolina
Our File # 1200.2242
Dear Mr. Butler:
Thomas M. Giller
Mark A Hester
William Paul Jones
Mark A. LaRose
Kimberley Marsh
Jose! D. Padilla
DeWayne A. Powell
Steven Robert Verr
Ot Counsel
Robert G. Wexler
This letter is to confirm our discussion of earlier today in which I requested any
and all documents relating to your department's investigation of the Channel Master site
in Oxford, North Carolina, including, but not limited to, the preliminary assessment and
site investigation reports. In addition, we request a copy of the draft HRS scoring for
the site. We understand that there may be a charge for copying this material. Please
contact me if this charge will exceed $100.00.
Please send the above-referenced material to my attention via Federal Express.
You may charge our Federal Express account: No. I 160-2868-9. Your prompt attention
to this request is appreciated. Please contact me if you have any questions.
TMG:cc
Very truly yours,
GESSLER, FLYNN, LASWELL, FLEISCHMANN,
HUGHES &. SOCOL, LTD.
~~
Thomas M. Giller
• •
12 November 1987
To: File
From: Jack Butler
Re: Telephone conversation with Jay Butler, Adams, McCullough, and Beard
(828-0564) about Channel Master, NCD 122263825
Mr. Butler contacted our office on this date to obtain information on
the Channel Master site in Oxford. A meeting was arranged for 2:00 p.m. on
Tuesday November 17, 1987. Mr. Butler agreed to prepare a letter requesting
access to the Channel Master file.
JB/pb/0520b.24
•
North Carolina Department of Human Resources
Division of Health Services
P.O. Box 2091 • Raleigh, North Carolina 27602-2091
James G. Martin, Governor
David T. Flaherty, Secretary Ronald H. Levine, M.D., M.P.H.
November 10, 1987
Koger Coats
Channel Master, Division of Avnet, Inc.
Post Office Box 1416
Industrial Park Dr.
Smithfield, N.C. 27577
SUBJECT: Cleanup of Channel Master Oxford, NCD122263825
Dear Mr. Coats:
State Health Director
A review of the data on soil samples from Southern Testing collected on
27 October 1987 reveals the following: Background soil from the Channel
Master site contains from 3.53 to 6.70 ppm total chromium with <0.05 ppm EP
Tax chromium. Composite surface soils from the base of the excavated
quadrants 3 and 4 on the west end of the former lagoon area contain 45.00 and
160.67 ppm total chromium respectively with 0.06 ppm EP Tox chromium.
It is understood that the bottom of the excavated pit is about 20 to 25
ft. below expected grade when the pit is refilled and leveled. It is also
w1derstood that the present excavation in the pit area addresses only metal
contaminants and does not address solvents contamination of the groundwater.
Tne site is presently undergoing review by EPA Region IV as a potential NPL
candidate.
Koger Coats
Novemoer 10,
Page 2
1987
•
After reviewing this information it is agreed that filling quadrants 3 and 4 on the west end of the former lagoon area with clean fill material would pose a minimum health risk. Sampling on 30 July 1987 of soil material removed from the top of this lagoon and stored along the Channel Master building and along the fence at the edge of the property indicates that this soil contains from 14 to 44 ppm total chromium. Based on this analysis by the N.C. DHR/DHS laboratory this soil appears to be acceptable as "clean" fill material. Sampling on 25 August 1987 of soil stored between these 2 piles indicates total chromium levels of 57, 64, and 182 ppm. This soil, soil to be removed from quadrants land 2 on the east end of the excavated lagoon, and all other soils presently stockpiled on site should be disposed of as a hazardous waste.
If you have any questions, please contact Jack Butler at [phone].
JB/pb/0489b.6
Sincerely,
~y~1~d
Solid and Hazardous Waste Management Branch Environmental Health Section
C. Department of Human Resources
.vision of Health Scrvicea
r ~6,,. -i\
• i •1~ .. rA~l\ V . ~QV State t:abon\ory of PubUc Health
SAMPLE ANALYSES REQUEST j§ 1 P. o. Box 28047
' ~ 306-N. Wilmineton Street
S Cf ~YASTI: N,1'$1/ · Raleigh, 27611
te Number .:::~::::::::::=:~'tl)~/.:...Z~7-:..::Z=:..:6~Jd. J::t:f'!...2::'.::.:._s--L __ Field Sample Number _.J_'f_Z_~_-________ _
ame of Site CA.a,;,,,.,:e/ /1ot rTe·y ---···_s;tc '--"-'on O x:;ra.Y"O(, /[/,,-C.,,-
ollected By
_____ _;_;;.:;.:.=:.._.,<; ...... .-.L-"-, ...... '--------....,...... >
.T, fi?, .$ M f / ~ Y ID/1 _'r"~~--Date Collected .S ~ T, /~I 'r J":Z Time /0 .1 · 0
rpc of Sample:
__ Groundwater (1)
__ Surface Water (2)
__L Soil (3)
__ Other (4)
Concentrate
__ SoUd (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
INORGANIC CHEMISTRY
Extracublca
Parameter Results mg/1 Parameter Rcsultsm&/1
,.,.,.-Arsenic ✓ n . O I -GArscnic <fi
LBarium < ,.-., ,OU-_Barium
✓Cadmium < 0. 01( ✓Cadmium < '/:.,0
-✓"Chromium <0.~Q --::;:;" Chloride
~Lead if:~s-__ Chromium '1,°K.
~j;~:, ___ _Copper
__ Fluoride
_-Silver <Q.~ __ iron
-✓ Lead :r.o
-__ Manganese
---✓Mercury--< o · l
-__ Nitrate.
-✓ Selenium '.5:0 -~~-
ORGANIC CHEMISTRY
Parameter Results mi/1 Parameter Rc&ults mg/1
_P&T:GC/MS _EDB
_ Acid:B/N Ext. __ PCB's
_TOX __ Petroleum
__ Endrin
__ -Llndane
MICROBIOLOGY
Parameter ParametCI'
_ (MF) Coliform Colonics/lOOmls __ Gross Alpha
_ (MPN) Coliform Colonics/lOOmls __ Gross Beta
Comments
Total
Parameter· Results m&ll
__ silver -<;. 1_0
__ sulfarcs
__ Zinc
-.Ph
__ Conductivity
_TDS
_TOC
------------
Parameter Rcault1 mg/1
__ Mcthoxychlor
--Toxaphcne
-2,4-D
--2,4.5-TP C•llvex)
RADIOCHEMISTRY
Rcaulta PCi/ 1
)ate Recciv~d ----------------Date Reported __ '/l-;--'A./-'---"-()--'t/'--_Jf_
7 _______ _
~epnrtcd By
)ar, Extracted------------~---Date Analy-.cd ----::--:--=:-:-------------
------------Lab Number __ 0_/_7_;4c..:./...:..4_,.Sc-aEP'-J'-'7_.,8....,7_--,-__
Location of Sampling:
DIVISION OF !ff.ALTtl SERVICES
SOLID.'D l!AZ.ARDOUS WASTE MA.NAG~T BIKH
Chain of Custody Record
Hazardous Waste Materials
Generator __ Transporter __ Treatment Facilit
__ Storage Facility __ Disposal Facility __ Landfill
VOther: C/i!!-a>t-U.(f?
Company's Name C ,/,;,,:1;te/ /3/'Qff er
Address Ox~,.,:,,( /!/4 C~
Collector's Name ~~✓
signature
Date Sampled S ez:12 T, /6=, / o/cJ 7 Tillle Sampled / 0.) 0
Type of Process Generating Waste . ...,.//".<:........:...;e=.l<c....:::a:..c/_--"t:P.-'-'./4"'a::...;._r_,_,,_~_c.n7 C¥'-------------• /
. Field Information
·Field Sample No. ?9'2.J"'
Chain of Possession:
.SM?/; IC:: l'Tf:7
inclusive dates
S""--4Aifl e, -/'}-f7
inc:lusive dates
3.
signature title inclusive dates
Instructions: Complete all applicable information inclcding signatures, and
submit ~ith·~nalysis request forms.
--, -
I
I
-1
I .,
I
I -•
W t&/1~,w o/ -5 p -:;-2,,_J 7#71/-5? @
~~'?;,~d.!~Jl~rv/5~/ 0 ~~5-o?.£ L :)I _Q --: : _
I -/;JI 6 ve-1-1 · :'.
TT~~) all ..
I
•
I
I
I
: I
I
• •
3U October 1987
ro: Lee Crosby
RE: Sampling at Cbannel Master, Nc:D122263825
On 21 October 1987, Jack Butler, N.C. CERCIA Unit met with Roger Coats,
Channel l"iaster, and Jeffrey O'Harn, Soil and Materials Engineering, at the
Ci1armel Master site in Oxford, N.C. Soil samples were collected for organic
and inorganic analysis at the surface and 1 ft. depth at the base of the
lagoon, at the effluent point from the lagoon, and at the surface and one foot
dept.ii at two background locations. All samples were collected by Soil and
Materials Engineering and split with Channel Master. Laboratory results are
pending.
jb/pb/U47Ub.15
. C. Department of Human ·Resources
,vision of Health Services •
ypc of Sample:
Environmental
__ Groundwater (1)
---a.....:,_· Surface Water (2)
V::::: Soil (3)
__ Other (4)
Concentrate
__ Solld (5)
__ Liquid (6)
__ Sludge (7)
--Other (8)
INORGANIC CHEMISTRY
Extractablea
Parameter
./ Arsenic
✓Barium
LCadmium
Lchromium
LL.cad
..L.Mercury
~~Jt.f'!iU.,tn _ ·-
_ Silver
Parameter
-. _ P& T:GC/MS
_ Acid:B/N Ext.
_TOX
--
Para.meter
Reaultsmg/1
o .rJ I
Reoults mg/1
MICROBIOLOGY
__ (MF) Coliform Colonics/lOOrnls
__ (MPN) Coliform Colonies/lOOmls
Parameter
..JL..Arsenic
..L....Barium
/Cadmium
__ Chloride
.,/ Chromium
--Copper
__ Fluoride
__ Iron
✓ Lead
----"7 Manganese
_✓_Mercury
__ Nitrate .
..JL..Selenium
Results miv
<4-,0
,:C7
/0
ORGANIC CHEMISTRY
Parameter
_EDB
__ PCB's
__ Petroleum
_Endrin
__ Lindane
Rcoults mg/1
Parametc,;
_ Gross Alpha
__ Gross Beta
Comments
So,'
__ Zinc
_Ph
OCT 28
__ Conductivity
_TDS
_TOC
Parameter
-. _ Mcthoxychlor
__ Toxaphene
-2,4-D
__ 2,4,5-TP (silvex)
--
RADIOCHEMISTRY
Reaulu mg/1
Rcoulu PCi/1
·" /o ,cL~-r':' %re Recdved _________________ Date Reported --'°'~""['-'---~""'-'-"l:::_ __ ~_f_'---------
)ate Extracted -------------~---Date Analy:ed ---,-,,-~-:-;-r-:-.r--,......:..-,-------
;: .:_:._,' : .__ ;_!__; .. : (. , ·-;
,;,ported By Lab Number ----------,---------
,,,,.. "''"' ,n ___ , __ .J-,tDC:\
. C. Department of Human Resources
1vision o( Health Sc-rvicc:1 "AMPLE ANALYSES REQUEST.· . State Laboratory of PubUc Health
P. 0. Box 28047
306 N. Wilmington Str«t
Raleigh, 27611
:te Number 3 r '1J I .2..,Z. 2 6 .J <f ;!. _s' Field Sample Numbet.:J"-'l,,._,'/.c.Ltf>'1...-________ _
ame of.Site . CAaaae-l ~ST¢';. ·,-s;tc Loa::ion O xz1,;o/, Mc../ ,
~ll~ct~d By Ve:( c.cf .d!Jur I e,y -ID/1 _..:.~-Y-"----Date Collected A9; .2 s;. 1 rcr 7 · Time / s-oo
ypc of Sample:
Environmental
__ Groundwater (1)
_._Surface Water (2)
~ Soil (3)
__ Other (4)
Extrac:tablca
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
INORGANIC CHEMISTRY
Comment&
So,1 l:,'/e
Total
Parameter Rcaults mg/1 Parameter Rcaults mvt<-J,-Parameter
..:::::...Arsenic <. '2. -'2. l LArsenic ~~ ./ Silver
✓Barium <Q,Q~ .L..Barium __ Sulfates
..LCadmium ~a.a'1 ✓Cadmium i-.~ __ Zinc
...JL...Chromium ~-~,_ __ Chloride _Ph
...JL...Lead .,/ Chromium z 9'~ __ Conductivity
...LMercury · __ Copper _ms
~~J~iu.rn_._ S::a ao~ __ Fluoride _TOC ~a. ;).o 7 1ron _-Silver ----_Lead t/J ----/Manganese < (2., --
-·-__ Mercury --
--__ Nitrate_ --LSclenium :!!:. o.~<;,.-----
ORGANIC CHEMIS'IRY
Parameter Re&ults mg/1 Parameter Rcaulamg/1 Parameter
___ P& T:GC/MS _EOB ___ Mcthoxychlor
_ Acid:B/N Ext. __ PCB's __ Toxaphcne
_TOX __ Petroleum _2,4-D
__ Endrin __ 2,4.5-TP (silvcx)
__ Lindane
MICROBIOLOGY RADIOCHEMISTRY
Rcaulta mg/~
< It">
Rcaultsmg/1
Parameter Paramet~ Results PCi/1
_ (MF) Coliform Colonics/lOOmls --Gross Alpha
__ (MPN) Coliform Colonics/lOOmls __ Gross Bera
Reported By
Oat< Extracted-------------~---Date Analy:cd -----,--;--"'.""'.'.""----,-:-:::-::-c:-:-:.,.,--------' I I ·'. ( ' / --.. f. I I ( r, .~ \!. I
_________________ Lab Number __ v_;_G_v_·_,_-.J_fi_~_,_,_L._·.,_~......,.,_. ------'--
[)HS 3 I QJ ( R('vi1oed 7185)
~il1J ;rnJ Ha~rdow Want" (Review 7/87)
. C. Department of Hum.an Resources
1vision of Health Services • • . SAMPLE ANALYSES REQUEST • Sutc Labonto,y of PubUc Health
P. 0. Box 28047
306 N. Wilmington Street
,--Rucigh, 2761 I
•
0
tc Number 3 Cf rt) I .2...2.. 2 6' 3 6'" .,Z-> Field Sample Number -'J~lf.,_I.,_'[ _________ _
amco{Sitc. ZAo,uie:I 8P' r&;.· ·:·s;teLocirion O ,xad, A/, C.✓ ,
~ll~ct~d By Uct C-6'. "$ uT I e,y lD/1 --'-f<~fr:,__ __ Date Collectccl A9 ~ 2 s;. I ro: 1 . Time / s-oo
ypc of Sample:
Environmental
__ Groundwater (I)
_._· Surface Water (2)
_.lL._ Soil (3)
__ Other (4)
Conccntriltc
__ Solld (5)
__ Llquid (6)
__ Sludge (7)
__ Other (8)
INORGANIC CHEMISTRY
Extracublco
Parameter
./ Arsenic
✓Barium
..L..Cadmium
...lLChromium
LI.cad
...LMercury ·
~l:;:u~--
· Results mg/1
< 0 ,DK: z t O a '(),02-
< a .oos-<o .}...O
Parameter
LArscnic
..,L.Barium
✓Cadmium
__ Chloride
✓ Chromium
__ Copper
__ Fluoride
__ Iron
✓ Lead
---;, Manganese
_,.,,.-_Mercury
__ Nitrate
L Scleni.,;,.
Total
Results mg/~ Parameter
Cl •f · ./ Silver G . __ Sulfates
:( y.o
/()
<o.,
__ Zinc
_Ph
__ Conductivity
_ms
_TOC
Results mg/~
ORGANIC CHEMISTRY
Parameter Rcoults mg/1 Parameter
___ P&T:GC/MS _EDB
__ Acid:B/N Ext _PCB's
_TOX __ Petroleum
__ Endrin
__ Llndane
MICROBIOLOGY
Pai-a.meter
__ (MF) Coliform Colonics/lOOmls
__ (MPN) Coliform Colonies/lOOmls
Date Recc:ivc;d ________________ _
Oat(' Extracted-------------~---
Reported By
[)HS 3 I QJ ( Rcvi..cd 7185)
~)l1J mJ Hi:.:irdous \VutC' (RC'viC'w 7/87)
Rcsulu mg/ 1 Parameter Rcaultsmg/1
-. _ Methoxychlor
__ Toxaphcnc
_2,4-D
__ 2,4S-TP (silvcx)
RADIOCHEMISTRY
Parameter; Results PCi/1
--Gross Alpha
__ Gross Beta
Date Reported ;;i_ <S Gcf ~z
Dare Analy:,ed
Lab Number
i ,,·_ .,_., f'
. . -,
DIVISION OF HEALTci SER\'ICC:S
SOLID AND 'HAZARDOUS llASTE HANAG~"J 5RAJICH
• Chain of Custody Record •
Hazardous ~aste Materi2ls
Location of Sampling: Generator __ Transporter __ Treat:Dlent ?2ci
Storage Facility __ Disposal Faciliry __ Landfill
Company's
✓Other: CE,:/€.C£A C/ean o/
N=eC/i'.«nne-/ -<'.1/a,5Ter Telephone(9'/?' ) €t.J-yC y,;?
d}r, 1 Ox:-&r:d'. &C, > z_7SC,C
Collector's Name(/~~-<
~ Signature
Date Sampled.Au q , ..2 S / f,?' 7 ../ J Time S=pled __ /_.)-_=:V---==0=------
Type of Process Gene:ating llaste~/7,::._,__c;,q.:.,_..Zf'--"q~· ~/ _ __,~'-L¼~a:,;_;rc....,_✓~-~7½9'.,,_ _________ _
_ Field Inform2-tion
Field Sample No. J-9'./7 ? 9'/J' 39/9'
Chain of Possession:
c':. tle
3.
signature title inclusive daces
Resul t.s
q(o C9-d-f1
date
Instructions: Complete tll applicable information incl~Cing signatures. and submit ~ith·~nalyiis request forms.
-.,ID
Locztic~ a: S2..I:l?ling:
DIVISION OF
AHIJ liAZARDOUS
Chain of Custociv Reco::-d
B2z2rdous ~2ste Y~te~i2ls
Generator
__ Storage Facility __ Dis?DScl Facility __ Landfill
/Other: CEtleC£A C/eat1 /412
Co.:ipany's N=eL/(rznn&I ,,8a,.51'er Tele?hOueW/7 ) 6:t'.. ?-YC' Yi?
Address Lu c/4 -.rTr ,-,.. I dJ,,,,,. ✓j OK TPro{. ,,A/, c_ z. 75£'. C
Collector's N=e ~~✓ Teleyho:oe(Y,1/9") 7JJ-,,Z,i"'O/ c7 Signature
Date Sampled Auy ✓ -2-; /'7,?'_7 Time S=ipledc......../_52c......::V::....e0::....._'--__
,Field Info:raE.tion
Field Sample No. Jo//7 j' 9'/J' _79/9'
Ch~in of Possession:
c':.cle
3.
signature tit.le inclusive dat.es
Instructions: Complete all applicable infornation incl~Cing signatures. and subw.it. \.:ith ·.analys~is request forms.
. C. Department of Hurru.n Roourcc:s
rvision of Health Sctvicct. • . SAMPLE ANALYSES REQUEST Sute L.bomcny of Public Health
P. 0. Box 280-47
306 N. Wilmington Street
Raleigh, 2761 I
·.teNumL-3C¥/fl /.2.22 6'.JJ'ZS--3a;a ucr I ~ Field Sample Number-~L~·~L ____________ _
amc ofSi~c . Z-Acu212e-l :'.'.'.%st?;. .,. S;te Locirion O ;;£},,,a( I MC✓ ,
~lle~~dBy Uotc.&-d!/llT/e,y. ID#---=-9_Y-"---DateCollcaedA9~ 2~.1rcr::t· Timc/000
ypc of Sample:
Environmenc.l
__ Groundwater (1)
_._· Surface Water (2)
~ Soil ( 3)
--Othc:r (4)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
--Othc:r (8)
INORGANIC CHEMISTRY
Comments
So,/ /./e
Extract:ablco Total
Para.meter
./ Arsenic
✓s .. _ anum
...L..Cadmium
..JL..Chromium
..JL..Lcad
...LMercury
~k-~iu..rn_._
_Silver
----·-
--
--
Parameter
___ P& T:GC/MS
__ Acid:B/N Ext.
~TOX
Panmetcr
· Results mg/1
s::o.ol
<'.0 ,0 t./-. < {) .Qli"
.(_ 0 -~ f_ l a Q -·o,o l.--
~ Q -~0.-~-
<6 ,l,.Q
Re5ulu mg/1
MICROBIOLOGY
__ (MF) Coliform Colonics/lOOmls
__ (MPN) Coliform Colonics/lOOmls
Parameter Rcoultsmg/~
L..Ancnic o.f=
..LBarium G.
✓ Cadmium :s: y_. C)
__ Chloride
✓ Chromium "G Y:
__ Copper
__Fluoride
__ Iron
✓Lead /tJ
✓Manganese __ Mercury <o . I
__ Nitrate.
..LSclcnium < C} .i~-
ORGANIC CHEMISTRY
Para.meter
_EDB
__ PCB's
__ Pc:rroleum
__ Endrin
__ Llndanc
Rcoults mg/ 1
__ Gross Alpha
__ Gross Beta
Parameter
✓ Silvc:r
__ Sulfates
__ Zinc
_Ph
__ Conductivity
_ms
_TOC
------------
Parameter
___ Methoxychlor
__ Toxaphcne
_2,4-D
__ 2,4.5-TP (•ilvcx)
RADIOCHEMISTRY
Resula mg/i,t.ff
"' /n
Results mg/1
Re<ults PCi/1
Date Recdvt::d
I ~7
----------------Date Reported -~~---:(,~_G~c'-"'l:~--'--------
Oat~ Extracted -------------~---Date Anal1-:ed ________________ _
Reported By _________________ Lab Number
OHS 3101 (R('VIK"d 7185)
~ili.l )r,J Hi:..Jrdou~ \X.'ntc (Rcvic'"' 7187)
. C. [?epartmc:nt of Hum.an Resources
ivi!.ion of He2lth Services • • . SAMPLE ANALYSES REQUEST Sme laboratory of Publlc Haith
P. 0. Box 280-47
306 N. Wilmi~on Street
R.,J<igh, 2761 I
.·te Numbcr 3 CJ'(/) 1.2.22 b 3 (5';?. ~ Fidd Sample Numbcr_..:J,<,..L.?;,._.'/£:;,__ _________ _
ame ofSite ZAaaae-1 c'.1/a-.s:T?r ··-.s;te Locii:ion O wd, Al, C..,, >
olle~~dBy Vac.,,f.,&uT/ey. IDll~~-zL~ __ Da,eColleacdA:5-9, .z~. 1ro:t:· Tune/<>0O
ypc of Sample:
Environmental
__ Groundwater (1)
-·-· Surface Water (2)
~ Soil (3)
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
C. CenTe,Y
INORGANIC CHEMISTRY
Comments
So,/ tf'/e
Extracnblcs Toal
Para.aietcr
./ Arsenic
✓ Barium
..L.Cadmium
..L Chromium
..LLead
...L..Mercury
~J~~iu_rn __
_-Silver
--
--
-·-----
. Parameter
-.-P& T:GC/MS
__ Acid:B/N Ext
_J"OX
Par-a.meter
Results mg/1
< t2 -Q l
<Q,Q~ < a,a"K'
~-~l_
~ a aoS.-
~Q.;}..o
Rcsulcs mg/1
MICROBIOLOGY
__ (MF) Coliform Colonics/lOOmls
__ (MPN) Coliform Colonics/IOOmls
Parameter Results m-vl<J-
...IL.. An;enic ¥ ~Barium li"
✓Cadmium <Y,..Q
__ Chloride
✓ Chromium z 9'.J....
__ Copper
__ Fluoride
__ Iron
✓ Lead 10
✓Manganese
__ Mercury ~o. l
__ Nitnte.
...JL...Sclenium ~ o ,'")__s-
ORGANIC CHEMISTRY
Pan.meter
_EDB
_·_PCB's
__ Petroleum
__ Endrin
__ Llndane
Results mEl'l
Paramctc.
__ Gross Alpha
__ Gross Beta
~aramctcr
✓ Silver
__ Sulfates
_Zinc
_Ph
__ Conductivity
_ms
_TOC
------------
Paxamctcr
-. _ Mcthoxychlor
__ Toxaphcnc
__ 2,4,D
__ 2,4,S..TP (silvcx)
RADIOCHEMISTRY
Rcsulcsmg/~
< / ,")
Raulamg/1
Results PCi/ l
Oa<c Exrracred -------------~---Date Analy:ed ---:--:--:-=--:-"'.":C"-::-::-7:--------
' I I: r, ... ~]!(:",--~'' _________________ Lab Number __ v_,_c.,_:...,_'_;_..J __ ~_,_._L_.,_-..,....·,_· -----~-!\cporred By
[)HS 3101 (R('vi-..::d 7185}
:=....11,..! .1.nJ H:i.:.udo~ 'J:'1stC' (Revie..,• 7/87)
•
21 October 1987
'lb: file
r'roru: Mary Giguere M0
Subject: Visit to Cnannel JvJaster
l~Wl22263i325
•
On Tuesday, October 27, 1987, Jack Butler and Stan Atwood are planning
to visit the Cnannel Master site. 1be purpose of the trip is to split
samples witn Channel Master. The samples to be taken are soil samples from
the bottom of the old surface impoundrnent. Sampling is to be conducted by a
contractor for Channel Master. Jack Butler and Stan Atwood are going to
observe sampling and accept the split samples. This work does not present an
innalation tiazard because CERCLA employees are not conducting sampling but
observing sampling from a safe di.stance. Level D protection is adequate for
this site.
H:X/ds/0479b.82
19 Oct. 1987
To: File
•
From: Jack Butler
•
Subject: Clean-up ;sampling at Channel Master, NCD 122263825.
Mr. Roger Coats,.Channel Master, contacted our office on this
date to reschedule sampling originally planed for this date. · .. The
sampling.was.rescheduled for 27 Oct. 1987.
. ' • • '\. C. Department o{ Hum.:m Resources
)i..,·ision of Health Services SAMPLE ANALYSES REQUEST
State Laboratory of PubUc Health
P. 0. Box 28047
306 N. Wilmington Srrcct
,itc Number .J o/d) I 2. 2 Z b J J-Z S"' Fielc\$'\ll}ple J:lum~L. J.L:(/ _______ _
lulcigh, 27611
Name of Site, _C_h_a-~"'="'~e,-~l~c/4__._~,q...._(~f~~r:~---------Site Locarion --0 6 7o· .,.c,,(J A!, C ,_.
:::Ollected By Ve J& f I Ov ID/I ~~-:i ___ Date Collected 7-JO-15' 7 Time _1_1/._,_, O_.;c.0_~
f ype of Sample:
Environmental Concentrate
___ Groundwater (1) __ Solid (5)
---Surface Water (2) ___ Liquid (6)
/ Soil (3) __ Sludge (7)
--Other (4) __ Other (8)
INORGANIC CHEMISTRY
Extractablea
Parameter
✓ Arsenic
✓Barium·
! ✓ Cadmium
/ Chromium
..£Lead
-/ Mercury
7 Scle_nium ..Zsi~er ----
Reaults mg/1
0.01
Parameter
✓ Arsenic
✓ Barium
✓ Cadmium
__ Chloride
._/ Chromium
__ Copper
__ Fluoride
__ Iron
✓Lead
__ Manganese
./ Mercury
__ Nitrate_
✓ Selenium
Reaulumg/
,q,
<o-iit3
Total
Parameter
-.i.::::::'."Silver
__ Sulfates
__ Zinc
_Ph
__ Conductivity
_ms
_TOC
Reaulu mg/J$f-
/0
ORGANIC CHEMISTRY
Parameter Results mg/ 1
_P&T:GC/MS
__ Acid:B/N Ext.
_TOX
--
--
MICROBIOLOGY
Parameter
__ (MF) Coliform Colonics/lOOmls
__ (MPN) Coliform Colonies/lOOmls
Parameter
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
Date Recdv~d ________________ _
Date Extracted -------------~---
Reported By
Results mg/ 1
.
Parameter
__ Gross Alpha
__ Gross Beta
Parameter Reaults mg/ 1
__ Methoxychlor
__ Toxaphene
_2,4-D
__ 2,4,5-TP (silvex)
--
RADIOCHEMlSTR'\.'
Resulu PCi/1
Date Reported ----+1_,_/J..::......,l'--"%'....i__r_J _____ _
Date Analyzed ---,--;--,-~7,,------:,,-,--------,: ,·' ·,. ; ·1 1: ;· . 1
,.JI "I,~'--~ ,,._:,. ,. 1. ·-~ ,,
Lab Number --------------:-----
I
' :
• •• ~-C. Oq,amncn't of Human Resources
Division of Health Services . SAMPLE ANALYSES REQUEST
State Labontory of Public Healer
P.O. Box 2804,
306 N. Wilmington Strcei
R.alcigh, 27611
s:ce Number J o/,1) / 2 2 Z b J J-Z S"' Fj;Jq $.:\!)}Pk ~u_mbg,=· ,,,.J.,...,o/,,.../,,., __ ...-.,.,7
..,_,-:-_ =-,,-------
Name of Si~ c,1,~'7He/ //4t rz:t!c -Sitel.oation ·o.x?p"..-q{J A(( c,..,
Collcaed By CT,, ifl« t/ c,v ID/I ~ '.7 Date Collect~ 7-3 O-6' 7 , ' ~~---
T yp,, of Sample:
Environmental
--Groundwatcr { l)
--Surface Watet (2)
✓ Soil (3)
--Other (4)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
INORGANIC CHEMISTRY
Commenu
Extracablcs Total
Parameter Resula mg/1 Parameter Rcsulamlf~ Parameter
~Arsenic .((1,/) ./ Arsenic O.s · ~Silver
✓ Barium ... ~ / n.o,~ ✓Barium ~ f" __ . Sulfates
✓Cadmium· ,:: I'") ,I') ,. ✓Cadmium <_,o _Zinc ..
/Otromium-. .-< ,., -~O __ Chloride _Ph
-'o/Lcad
"· .. !!::'./..-01> ✓ Chromiw:,; lY ... _._._· Conducti."vicy .
:< Q • 0 :,;)..__ Copper _IDS Mercury ✓ "-leniurn · · ./ r, r,/)~ __ · Fluoride ._Toe
LS!lve~ ---:( '2-N:> __ Iron --
--✓Lead ~-0 --
--__ Manganese --
-·-✓ Mercury :S::::Q,I --
--__ Nia-ate. --
--✓ Selenium <CJ.~~---
ORGANIC CHEMISTRY
Parameter Results mi" 1 Puameter Rcaulta mg/ 1 Parameter
_P&.T:GC/MS _EDB __ Methoxychlor
_. _ Acid:B/N Ext. __ PCB's __ Toxaphcne
_TQX __ Petroleum _2,4-D
--_Endrin __ 2, 4 ,5-TP ( silvex)
--__ Lindane --
MICROBIOLOGY RADIOCHEMISTRY
Rcaulamg/~
<./0
Rcaulam&fl
Parameter Pan.meter Rcaula PCi/1
__ (MF) Coliform Colonies/lOOmls
__ {MPN) Coliform Colonics/lOOmls
--Gross Alpha
__ Gross Beta
Dace Receiv~d ---------~------Dace Reported --r7--:_-"'0:'-'---"/:..._ __ f'_; ______ _
Dace Extracted---------------'----Dace Analr..cd --;.---;-, --:-.-;,7"'.", .--:---:--;-------
v. i 1; ; u: 1,}1... l ..• ,_ ••
Reported Bv ________________ Lab Number ----------------
' . • • '>. C. Dcpamncnt of Human Resources
:livi.sion of Health Sctvlca SAMPLE ANALYSES REQUEST
State Laboratory of PubUc Health
P. 0. Box 2804 7
306 N. Wiunington Street ·
5;tc Number Jo/tf)l2Z ZC JJ-Z 5"' Fj;Jd,$.:\~pl_s~\lIDl,g,, J_Z{ ~-'"--..
Raleigh, 27611
l'<ame of Si~ Cha,z,-,e, / ./f,q (Tt!r: -·Site Location. o; .• {7.o.,--o/J Wt c.,_ . -
Collected By v,,lkT/°f" IDll~,.:_y ___ Dace Collected 7-Jo-J-7 ·• Tune l!:zo
i ypc of Sample:
Environmental
__ Groundwater ( 1)
__ Surface Water (2)
✓ Soil (3)
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Ocher (8)
Commcnu
INORGANIC CHEMISTRY
Extractables
Parameter Reaulta mg/1
..:::::....Arsenic <~ ,0 ,·
__.:::::.Barium -~:~--:?Cadmium __ Chromium
~Lead s: t..,aa
Mercury s::: Q,Q-;).......
7 Selenium -<. Q. oos.-
ILsi!~~ ----< (). d-0
-----------
Parameter Resulumg/1
_ P&. T:GC/MS
_ Acid:B/N Ext.
_TOX
----
MICROBIOLOGY
Parameter
__ (MF) Coliform Colonics/lOOmls
__ (MPN) Coliform Colonics/lOOmls
Total
Parameter Resula mg/l(f-Paramttcr Results mg/l<e_
-Arsenic /, () · ~Silver </0 v.
✓ Barium 7;... _. Sulfates .
✓Cadmium < -q_. () __ Zinc :,. •.
_Chloride _Ph
./ Chromium .'.JS-_--_Conductivity·
_Copper _ms
__ Fluoride _Toe
__ Iron --✓Lead ~-() --__ Manganese
✓ Mercury ~(")., --__ Nitrate. --
✓ Selenium ~(2_-~~---
ORGANIC CHEMISTRY
Parameter
_EOB
__ PCB's
__ Petroleum
__ Endrin
__ Llndane
Resnlumg/1
Parameter
--. Gross Alpha
__ Gross Bea.
' Parameter Resulta mg/1
__ Methoxychlor
__ Toxaphcne
_2,4-D
__ 2,4,S.. TP (silvcx)
--
RADIOCHEMISTRY
Resulu PCi/1
.. -----------
Date Received ---------'---------Dace Reported --7t:_~t};~c._...f_· _f_-;7 _______ _
Dare Extracted Dace Analr..cd --"TT-,--,--,-~--,--,------·__;;{~ ,:e;.~ J~.--... ·-)-./,
________________ Lab Number -------------,----
• i. C. Department of Human Resources
ijvJsion of Health Scrvicca SAMPLE ANALYSES REQUEST
State Labontory of Public Hc2.lth
P. 0. Box 2804 7
306 N. Wilmington Strett
;;tc Number Jo/d)/.ZZ ZC JJ!-Z _s-" Fi~c!.AAmpl_sJ:,µmbc;r,. ]__Cf l_f ...... .
Raleigh, 27611
~•me of Si~ C/4~,,.,,,e/ /-ta fft:.r -Site Location O,x.;zJ;.,ty(J A!, C'<-
::OllectedBv Vcdl«f/c,,,, ID#_,_2':_:f,.__ __ DateCollected 7-Jo-J-7 ·• Tune /(,'JO
r ype of Sample:
Environmental Conccnttate
--Groundwater (1) __ Solid (5)
--Surface Water (2) __ Liquid (6)
/ SoU (3)
__ Other (4)
__ Sludge (7)
__ Other (8)
7#F
INORGANIC CHEMISTRY
Extr.actablea
Parameter
✓ Arsenic
~Barium
'✓ Cadmium
17Chromium
LI.cad -7 Mercury
Parameter
Arsenic
-;::7 Barium
✓Cadmium
__ Chloride a,.o
Commenu
Tow
Parameter
--Zinc
_Ph
__ Conductivity ·
_ms
✓~~it!!_n __
-/Chromium.
__ Copper
__Fluoride
__ Iron
______ ._Toe
-Silver
-· -------------
Parameter Results mg/1
·-P&.T:GC/MS
_ Acid:B/N Ext.
_TOX
----
MICROBIOLOGY
Parameter
_ (MF) Coliform Colonies/lOOmls
__ (MPN) Coliform Colonics/lOOmls
../Lead
_Manganese
✓ Mercury.
___ Nitntc_
✓ Selenium
7.0
<22,,iZ j
ORGANIC CHEMISTRY
Parameter
_EDB
_PCB's
__ Petroleum
_Endrin
__ Llndane
Results mg/ 1
Parameter
__ Gross Alpha
__ Gross Beta
Parameter Reaultsmg/1
__ Methoxychlor
__ Toxaphene
-2,4-D
__ 2,4,5-TP (sUvex)
--
RADIOCHEMISTRY
Results PCi/1
Date Recciv~d ________________ Date Reported ---+7-0i=-_;,J--~,'---!(_J ______ _
Da« Extracted Date Analyzed ----:-----:------------, : ; ' ' . ·: i' ': . ·: . :,. '
Reported By _________________ Lab Number __ . __ ._, _.,_,_'-'_'-'_~_,_._· _,_. ___ ,_; _______ _
.
N. C. Department of Human Resources
Division of Health Services
• ••
. SAMPLE ANALYSES REQUEST
State Laboratory of Public Heald
P. 0. Box 2s04·
306 N. Wilmington Stm
S;teNumbcrJo/d)I.ZZZCJtfZ_s---' Fid4$o..rt}pk~~bg,_ ~ °l!S: ..... . R..leigh, 2761
Name of Si~ Ch~.,,,,, e I da t-1: t! c -Site Loa:ion . O .x -7I; .-o-1) A(/ C:,., --·
Collected By J:. <1f« f/ Of" ID# ~'/-_7:.,..__ __ Date Collected 7-JO-J-7 Tune //, '7'-0
Type of Sample:
Environmental Concentrate Commenu
Groundwater ( 1) Solid (5)
Surface Water (2) Uquid (6)
✓ Soil (3) Sludge (7)
Other (4) Other (8)
INORGANIC CHEMISTR.Y
Extnctablcs Total
Parameter Resulu mg/1 Parameter Rcsnla me/""....-Parameter Rcsulume,'~
✓ Ars,: • < n.o I Arsenic: I.;') · ~Silver ~i. 0
-rue
...::;:::: Barium • ·, <i"l ,.., IL ✓Barium G,.O ~Sulfates
✓Cadmium·· .c' r) /I}{ ~Cadmium < l/-, 0 _Zinc;
/ Chromium s:: a .1.£) __ Chloride . -Ph
~Lead < t.' 12. " ✓Chromi~ ?-.!J: _._· Conductivity .
Mercury.·· s:·a .Q~ __ Copper _ms
, ✓ ~len_i~~ ·_ ~ Q, QQ~ _•_fluoride _TOC
Lsilve, .S::::: C1 • .;bQ __ Iron --
--✓Lead &'tz ·Q --
,., ·~ .. __ Manganese ----
-·-✓ Mercury <12..l --
--__ Nitrate. --
--✓ Selenium < 0. ;;.s---.
ORGANIC CHEMISTRY
Parameter Rcsulu me/1 Parameter Rcsula me/1 Parameter Rcsulta mg/1
_P&.T:GC/MS _EDB __ Methoxychlor
-Acid:B/N Ext.. _PCB's __ Toxaphcne
_TOX __ Petroleum _2,4-D
--_Endrin __ 2,4.S-TP (1Uvex)
--__ Undane --
MICROBIOLOGY RADIOCHEMISTRY
Parameter Parameter Rcsulta PCi/1
--(MF) Coliform Colonics/lOOmls
--(MPN) Coliform Colonies/lOOrnls
__ Gross Alpha
__ Gross Beta
Date Receiv~d ----------'--------Date Reported __ 7"--;-__,_U,"'--',....,t:"-_· _'?_· _7 ______ _
Date Extracted Date A=lyzcd ----,:--:------------, I I · .
\.._..,' j /~ I(_;.·:. 11 :_; •'~' \' I
Reported By ________________ Lab Number _______ v_,._,··~•--... · "-'~"-'-'-• ____ _
.
• ~-C. Department of Human Roources
Division of Hcalth Services SAMPLE ANALYSES REQUEST
State Laboratory of Public Hcalc
P. 0. Box 2804'
306 N. Wilmington Str«
Raleigh, 2761
Si.re Number J o/d) 12 Z Z b .J J-Z S---] '11(; Fidc!~mpl..s_~u-~bq=· ==...,.,..,. ~=-==-,_..... ______ _
Name of Site _C_J,~Cl'~tz~"-e~/~/-ft~~a~~r~r~~~c _______ -Site Loarion O i 71 .,..o-f) A,,,, C ?,
Collected By v,, elk T / 6 v ID# --'-~---'L-j-___ Date Collected 7-JO-J'-7
Type of Sample:
Environmental
--Groundwater (1)
__ Surface Water (2)
/ Soil (3)
__ Othcr (4)
Extractablcs
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
INORGANIC CHEMISTRY
Comments
TotllJ
Parameter Results mg/1 Parameter Results mi/19'-" -· Parameter Raultsmg/1~
, ✓ Arsenic ~0-°g_ ../ Arsenic /, v--Lsilvcr <LD
,/ Barium _a, a ../ Barium ·pb __ sulfarcs
./ Cadmium <.Q.rJ!s ✓Cadmium <. LJ.., 0 _Zinc
• / Chromium ./Q,.:l..O __ Chloride __ Ph
~Lead -< l.£ 0 c1 ../chromium 44 __ Conductivity ·
Mercury <rJ1D~ __ Copper _ms
~ 7 Selenium <Q,Ot?S: __ fluoride _TOC
-..L s~~e~ ---< 0 . .)_Q __ Iron --
--./ Lead II --
--__ Manganese --
--✓ Mercury <0-1 --
.. __ · Nitn.te ----
--✓ Selenium :S:Q. l;< --
ORGANIC CHEMISTRY
Parameter Results mg/ 1
_P&T:GC/MS
__ Acid:B/N Ext.
_TOX
----
MICROBIOLOGY
Parameter
__ (MF) Coliform Colonics/lOOmls
__ (MPN) Coliform Colonics/lOOmls
Parameter
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
Rcsulu mg/ 1
Para.meter
-. Gross Alpha
__ Gross Beta
Parameter Results mg/1
__ Mcthoxychlor
__ Toxaphene
-2,4-D
__ 2,4,5-TP (silvcx)
--
RADIOCHEMISTR)"
Results PCi/1
2 c)c--~ ,YJ
Date Received _________________ Date Reported ---"'"-;--__.__---'J___'------------
DatC' Extracted-------------~---Date An.aly--..ed ---;;-;--:--::-------------, '
Reported By _________________ Lab Number __ ,_'_,_' _'-_•,_-'_,_·_~-"-~-------
DIVISION OF HEALTH SERVIC:::S
SOL Ir HAZARDOUS WASTE MANAG~T e1'CH
Chain of Custody Record
Hazardous Waste Materials
Location of Sampling: Generator __ Transporter _Treatment Facili·
__ Storage Facility __ Disposal Facility __ Landfill
v Other: C /earlU,Q
[/
Company's Name c;; crr11-1e/ ./1/'a cf'ey Telephone( C//'f) £ 'l3-'f-6'(0
Address C .x -/"a-rd /[/', C /
Collector's Name ~~
~ signature
Tele_phone( o/l'f) "13 J-:Z.,?O/
Date Sampled ·'CJ;., o/ .J ';• lo/Jl"/ Ti.me Sampled 1/-/,Z ,'00'
Type of Process Gene~ating Waste ..... c::::½~1...•..:ce::::..<..&""-'/c.._....1.£.,_.1/,:...:a,:;,;...:-f,....;..., '.:..n-':,_,, D/..,_c.....:J;:;;;...c;l,..r.fl:,..~";'-;e>;< ... e:::.,,,.,,."'------
. Field Information
Field Sample No. J 'r I/ 'J· 'f I ;z.. 'J'f /,J-3 ii¥
Chain of Possession:
1.
'-~-~ . · signatury
7-J"O-v-J /-J"_7
inclusive dates
3.
signature inclusive dates
Results ;:;ze~./ g
signat~ ~~
Instructions: Complete all applicable information incl"ding signatures, and submit ~ith·2nalysis request forms.
To:
From:
Subject:
• •
09 October 1987
File
Jack Butler
Telephone conversation with Roger Coats [phone] concerning
Channel Master, NCD122263825
Mr, Coats contacted our office on this date to reschedule our
sampling visit for from 12 October to 19 October 1987.
JB/ds/0479b.40
l::."OC'parr.ment o{Human Resources
t'-:isio~ of Health Services •
• · • State Laboratory of Public Health AMPLE ANALYSES REQUES P. o. Box 28047
306 N. Wilmington Street
Raleigh, 27611
·« Number J Cf rt) / 2,2. 2 6' J cf;?. _s" Field Sample Number .=J:.....::.6'....;7____::.1 _________ _
ame of Site . CAaaae:I c:% .s:t~t:: ·:.· Site Lociirior. 0 xt'Jd , M C-,, ,
~lle~~dBy Uctc~-d!];;r/er ID#____::.9_..L..Y. __ DateCollea«1A9 ✓ 2~, lo/ct7· Time/<>0O
ype of Sample:
Environmental Concentrate If Co
Ce~T-PY /4 :'M: I,;~/~'... __ Groundwater ( 1) __ Solid (5) I -\ _._Surface Water (2) __ Liquid (6) I ' ~ Soil (3) __ Sludge (7) ::r:
~
N OCT 9 19Jl7 :,: __ Other (4) __ Other (8) "' 0 ~
INORGANIC CHEMISTRY '{& r /:-n ~·' • ~ '" To~ .. ,<,~/ Extractablcs ,\{',
Parameter Results mg/ 1 Parameter Rcsultamg/1 'p,.Jji~~ Rcsulumg/1
_Arsenic __ Arsenic __ Silver
_Barium __ Barium __ Sulfates
_Cadmium __ Cadmium __ Zinc
_Chromium __ Chloride _Ph
_Lead __ Chromium __ Conductivity
_Mercury __ Copper _TDS
____ Selenium_·-__ Fluoride _TOC
_-Silver __ lron --
-_Lead --
-__ Manganese --
--__ Mercury --
--__ Nitrate --__ Selenium ----
ORGANIC CHEMISTRY
Parameter Results mg/1 Parameter Results mg/1 Parameter Rcaulumg/1
P&T:GC/MS _EDB ___ Mcthoxychlor
✓ Acid:B/N Ext. __ PCB's __ Toxaphcne
_TOX __ Petroleum _2,4-D
__ Endrin __ 2,4.S-TP (&ilvcx)
__ Lindane
MICROBIOLOGY RADIOCHEMISTRY
Parameter Paramete,; Results PCi/ 1
__ (MF) Coliform Colonics/lOOmls __ Gross Alpha
__ (MPN) Coliform Colonics/lOOmls __ Gross Beta
o .,,/ o-7 c,-.Jo -J 7 Date Received ------"IL'----'ol"'-'-o"---_..(Lc..,__:fU=,..Jj.._-______ Date Reporred ---:--'-7_:::_ __ __::..._ _______ _
Da« Extracted _q'--,...,_/_,-~'--/--r'-· ~7_.,6.,_.,/J'--_----~---Date Analysed _9,__-,.../""'S--;-:;:t~7:-;;;;,6';-~;:::-;::---------~ ,:? A.L -/ 7(lZ283
~4"~=:....:....<:.....:;..,.--'?r:_-'-----'~'-'-----Lab Number ------------,----:----'---( .
'FT7D2-2 r _;>-7D Z...2--,f-S-
Reported By
[)HS 3 I 01 I R("\'iKd 7185)
~,l,J ,mJ H;i.~rdous \X'utc-(Revie"'1 7/87)
. c:·D.eparpnent o{Human .Resources
:l,'.isiOn of Health Services .AMPLE ANALYSES REQUES.
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 2761 I
.·,e Numbc,r Jo/ rt) I ,2..,2.. 2 6' J cf .,Z 5" Field Sample Numoo _,'J"'-"C<...L7.....;:;.<f>' _________ _
ame ofSire . ZAaatie-l <'.o/'a-s:~r ·,.· Site Lociinon O x79,eol,, M C-,,,
ollectedBy Vctc/:",$;./7'-/e,y IDll~9_Y.~--DateColleccer1A9 ✓ 2-s-, 1cro:7· Time/S"0O
ype of Sample:
Environmental
__ Groundwater (1)
_._· Surface Water (2)
___i.:::::::_ Soil ( 3)
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
C
INORGANIC CHEMISTRY
Extractables
Parameter Results mg/1 Parameter Results mg/1
__ Arsenic __ Arsenic
__ Barium __ Barium
__ Cadmium __ Cadmium
__ Chromium __ Chloride
_Lead __ Chromium
__ Mercury __ Copper
----S~k~iuJn ___ __ fluoride
__ Silver __ Iron
--_Lead
--__ Manganese
--__ Mercury
--__ Nitrate
__ Selenium --
ORGANIC CHEMISTRY
Parameter Rcsultsmg/1 Parameter Resulumg/1
/ P& T:GC/MS _EDB
__ Ac1d:B/N Ext. _·_PCB's
_T0X __ Pcrrolcum
__ Endrin
__ Lindane
MICROBIOLOGY
P~rametcr Parametc~
Comment&
So,/ c£,Je
Total
Parameter Resulumg/1
__ Silver
__ Sulfates
__ Zinc
_Ph
__ Conductivity
_TDS
_T0C
------------
Parameter Rc,sultsmg/1
-. _ Mcthoxychlor
__ Toxaphcnc
__ 2,4-D
--2,4,5-TP (&ilvcx)
RADIOCHEMISTRY
Results PCi/ 1
__ (MF) Coliform Colonies/lOOmls --Gross Alpha
__ (MPN) Coliform Colonies/lOOmls --Gross Beta
Dare Received ___ ?u..:·:s:~.t.)~(o"--'-'15''--7.L.___,'77,J.,IJ'-"'=-------Date Repon:ed ---;----------------
Dare Extracted _9.,__-/'-"..),,_-_-..;eff_7,_,_/3=J"------~---Dare Anal1=d _ _,_9_✓..,_/..,.·J ... -.-~i;;:;7;-:;;-;3~)]~;---------702284
Reported By __________________ Lab Numoo
OHS )JQJ (Rc-vis.ed 7185)
~1,J ~nJ H;i:.udou.s Wutt" (Revic-w 7/87)
. C: Dcpai;nncnt of Human Resources
1yisiOn of Health Services .AMPLE ANALYSES REQUES.
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611
te Number _J_o/'-"'@~/'-2-=-,Z._Z_6"_.J_cf_,Z_S' _____ Field Sample Number ..:.J'~C:-· L7~9 _________ _
ame of Site · CAanae,/ .,Az'.a, .S:Z:'.~r. ··· Site Location O ,g,(],,,a(,. MC-/
~Ilect~dBy Vctc&·g;_;-;-;e,y ID#____:_~_..L..y. __ DateCollectc<ld09~ .2~. icro:7· Time/<>0O
ype of Sample:
Environmental
__ Groundwater (!)
_. _ Surface Water (2)
~ Soil (3)
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid ( 6)
__ Sludge (7)
__ Other (8)
vlcenTeY
INORGANIC CHEMISTRY
Extractable& Total
Parameter
__ Arsenic
__ Barium
_·_Cadmium
__ Chromium
_Lead
__ Mercury
---S~k~iu_!11 __ _
__ Silver
Parameter
_P&T:GC/MS
✓ Aeid:B/N Ext.
_TOX
Parameter
Results mg/1
Results mg/1
MICROBIOLOGY
__ (MF) Coliform Colonics/!OOmls
__ (MPN) Coliform Colonics/lOOmls
Parameter
__ Arsenic
__ Barium
__ Cadmium
__ Chloride
__ Chromium
__ Copper
__ fluoride
__ Iron
_Lead
__ Manganese
__ Mercury
__ Nitrate _
__ Selenium
Re&ults mg/ 1
ORGANIC CHEMISTRY
Para.meter Results mg/1
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ Llndane
Paramctc~
__ Gross Alpha
__ Gross Beta
Parameter
__ Silver
__ Sulfates
__ Zinc
__ Ph
__ Conductivity
_ms
_T0C
Parameter
-. _ Methoxychlor
__ Toxaphene
_2,4-D
--2,4,5-TP (silvex)
RADIOCHEMISTRY
Reaulumg/1
Rcsultsmg/1
Resulu PCi/ 1
-----'9,__-_.,.,_),._.(n"'-·...1.5?L...J.7'---'7...Lt.2""1&'-'I::-----Date Reported ---;---------------
Date Extracted _CJ.f..._~!..../:,1.J_-....!}'!....7.!.....'.(3"'--'&::;:_ ____ ~---Date Analy:cd _C/-'---~i~:(~-~!(~7'--"--'A"'.&='---------
Date Receiv~d
Reported By ---------------Lab Number ___ ___..&7wO..w.:2u2 ...... Bz...r.l.b,-. -----'--
DHS 31QI fRevi.c:d 7185)
S.ObJ .anJ Ha.~rdou1, Wutc-(Review 7 /87)
. '
DIVISION OF HEALTH SER\'IC:C:S
SOL. AND RAZARDOUS WASTE MANAG::!-SK~CH
Chain of Custody Record
Bazardous Waste Materials
Location of Sampling: Generator Transporter __ Treatment Facil:
__ Storage Facility __ Disposal Facility __ Landfill
✓Other: CEt:leCL'A C/ecw ~
NameLAa11ne/ ./1/'a,5~y Telephone(9'/r ) er. l-~6 y;:J Company's
a!Jr-, 1 Ox:z?ora{. ,d/4C_ z_ 7 .... "CC,C
Collector's Name~-< = signature
Tele_phone('V'9') 7.3J-~,i""O/
Date Sampled Au~, ,,2 S I ft?' 7 _r 7 ; Tilne Sampled;.._/_..>_-..;;v:....:O::._ ___ _
Type of Process Generating Waste/1/e °Lq / ~ /a r',, 'o/
. Field Information
Field Sample No. J €:7 7 3 o7cJ" JC79' __ _ '
Chain of Possession:
1. <2-t;v/4/1u~
O' signature tffle
,4 q ,r, 7-S--,, .,Z ( l'/?7
in<lusive dates
2.
signature inclusive dates
3.
signature title inclusive dates
Rescl:s reported
signature title date
Instructions: Complete all applicable information inclucing signatures, and submit ~ith ·3nalysis request forms.
• STATE LABORATORY Of PUBLIC HEALTH •
DIVISION Of HEALTH SERVICES, N.C. DEPARTHENT Of HUHAN RESOURCES
P.O. BOX 28047 -306 N. WILHINGTON, ST., RALEIGH, N.C. 27611
ORGANIC QjEHICAL ANALYSIS
BASE/NEUTRAL AND ACID LAB NO r/tJZZ.9, '< ,022p,t/ 702-zH.;;
EXTRACTABLES FIELD# 3&77 _3(,,,'7 J/ 7b7'7
COHPOUND TYPE ( ~ l ( -\ ( ~ 1 ( )
UNITS .. n/J t.',n/l(n ,on/ 1 ,n/knJ ··"/1 f.n/i(a un/1 un/kQ
N-nitrosodimethvlamine ..,.. 0 "'-'-<-1.-<-
bis(2-chloroethvllether
2-chlornnhenol
ohenol
1 3-dichlorobenzene
1 4--dichlorobenzene ~ 1.2--di ch lorobenzene
bis(2-chloroi llether
hexachloroethane
N-nitroso--di -n-n~v]amine
nitrobenzene
lsrvi.horone -· ·-
2-nitrnnhenol
2 4--dimethvlnhenol
bis(2-chloroethoxvlmethane '
2 4--dichlornnhenol
1.2.4-trich lorobenzene
naohthalene
hexachlorobutadiene
4-chloro-<n--eresol
hexachlorocvcl=ntadiene
2 4 6-trichlo~henol
2-chloron>nhthalene
acenaohthvlene
dimethvl ohthalate
2 6--dinitrotoluene
acen;mhthene ,.
2.4--dinitrnnhenol 11,.,I>
2.4--dinitrotoluene "I=?,,.,
4-nitroohenol I (p .'>()
fluorene -~.::Zn
4-chlornnhenvlohenvlether 3=10
diethvl ohthalate 33,,
4.6--dinitro-o-cresol /b ._-ii
diphenvlamine Jt'~.<l>
azobenzene j/h\o
4-braroohenvlnhenvlether _ • ., 0
hexachlorobenzene =i_-=? c)
DPntachlorCV\henol J ;_ ,-,;
ohenanthrene ➔ °C?O
anthracene -::i ~ (.)
dibutvl ohthalate ~ 'lo
fl uoranthene ; 2,·J 'I o/
J -Estimated value. K -Actual value is known to be less than value given.
L -Actual value is known to be greater than value given.
U -Haterial was analyzed for but not detected. The nutber
NA -Not analyzed.
is the Hininun Detection Limit.
1/ -Tentative identification.
~I -On NRDC List of Priority Pollutants.
N. C. V,i_v,W,i_an 06 He.a,Uh SVtv,i_cv.,
VHS 3068-0 14/86 Laba~a,ta~y)
-
( ) ( )
.. n/1 .. n/ka ,on/ 1 ,on/kQ
• • STATE LABORATORY Of PUULIC HEALTH
DIVISION Of HEALTH SERVICES, N.C. OEPMTMENT Of HUMAN RESOURCES
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC OlEMICAL ANALYSIS
BASE/NEUTRAL ANO ACID LAB NO 7o2ZJl3 7022.IJ<I 7022$5"
EXTRACTABLES FIELD# J(o77 . :?(o 78 :?✓-79
COl1PWNO TYPE ( 3') ( <) ( :?) ( )
UNITS ,,nf l '"-nika .. n/1 ,:;./k-;;-l ""/ l ✓.".'n/knl ,on/ I ,on/kQ
nvrene 3"? D ·rA.,; l,,C l-L.
benzidine /{;Sc)
butvl benzvl ohthalate =i:::io
benz(a)anthracene =l=lO
chrvsene '>'~O
3.3-<lichlorobenzidine ,, C/l
bis(2-ethvlhexvllnhthalate '1.3 0
di-n-octvl ohthalate 3~ 0
benzo(b)fluoranthene 16.CO
benzo(klfluoranthene
benzo(a)nvrene
indeno( l 2 3-cdlnvrene
dibenzo(a h)anthracene
benzo(a h i l=rvlene .., ,. / , -.
aniline //,.CV lA...-U-i..,L.
benzoic acid I
benzvl alcohol ,J,.
4-ch 1 oroan i 1 i ne 330
dibenzofuran
2-ll'<!thvln•nhthalene
2-ll'<!thvlphenol
4-ll'ethvlohenol ✓/
2-ni troani line / /. ,-zi
3-nitroaniline
4-nitroaniline
2.4.S trichloroohenol • /1 . , 'j. .,
/h]JL
-. -~ _.. ~-II
II
J -Estimated value. K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. u -Haterial was analyzed for but not detected. The nunt>er is the Minioun Detection Limit.
NA -Not analyzed.
1/ -Tent.alive \dentificat1on.
~I -On NROC List of Priority Pollutants.
N. C. D-i.v,0.,-i.on 06 1/eaUh SVJ.v-i.ee/2
DHS 3068-0 (4/86 LaboM.t.011.11)
( ) r )
ua/ I .. n/ka .. n/ I ""/ka
. I
C. bcpar~~:\t of,l-iu'rnan Resources
.•;,.,on,of H:alch Servic .. . s&LE ANALYSES REQUEST • State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmingu,n Street
Raleigh, 27611 .. ,
e Number J'(,1)/22ZCJJ-Z S"
:-:,eofSire Ch,:;i,n,-,e Ida r-fl!c
Fis:ld.MIT}Pk ~1.1.ffi~-=·· ,;;;~;.,,._ ·,,,.6...;;, ~""-~"'=-=·-:-,--==-=------
-Sire I,.oca:ion .· 0 i 71 ....-o/J A!✓ C >-, --· .J .
,ilected By _V-=--,cc.:df...._.a"-,_T-"-/=t:,v~---ID# ~"-:f-• __ Date Collect~ 7-JO-tf 7 Time ///00
0 of Sample:
c~v1ronmen tal Co ncenttatc Co mmenra
__ Groundwater (1) Solid (5) / c!3 /\\ECE~
.. / ·. '{I'\
__ Surface Water (2) Liquid (6)
v/
l::i:: ' Soil (3) Sludge' (7) h
'"' ocr 9 :P jon~
Ocher (4) Other (8) ?CJ
Q CJ
INORGANIC CHEMISTRY ~~ CERr.1 ' _0-{;/
Exttactablea Total~l'r.
~ . _.,"<'V
Parameter Results mg/1 Parameter Results mg/1 p '-,,..lrfl--<.11.j A.\..it.1/ arameter~ Rcaulumg/1
_Arsenic __ Arsenic __ silver
_Barium __ Barium __ Sulfates
_Cadmium . __ Cadmium __ Zinc.
_Chromium __ Chloride _Ph
__ Lead __ Chromium __ Conductivity
.. __ Mercury __ Copper _TDS
___ 5;ekniuJ_n ___ __ Fluoride· _Toe
_ Silver _Iron --.. _._Lead,·:, ..... ---••:;~. ~-~~.--·:_, .•·;-_Manga~, ----__ Mercury --·--__ Nitrate. --
-_Selenium --
. ,-! .. • . . ....... ,
ORGANIC CHEMISTRY
Parameter Rcaulumg/1
__ P&T:GC/MS
JL Acid:B/N Ext.
_TOX
·--·-:-;
MICROBIOLOGY
Parameter
__ (MF) Coliform Colonics/lOOmls
_ (MPN) Coliform Colonics/lOOmls
Parameter
_EOB
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
Reauhs mg/1 Parameter Rcaulumg/1
__ Methoxychlor
__ Toxaphcne
__ 2,4-D
--2,4,5-TP (silvcx)
--
RADIOCHEMISTR'¥
Parameter Results PCi/1
__ Gross Alpha
__ Gross Beta
Dare Reported /()-Z ·-,?-7 !PJJI -.
Date Analy:ed 'i-17-8@
Lab Number ___ ?_0_Z_0_1-_.\ ___ -:----
:. Department of Hil.~n Rcsourcos
ision ,<>f Health Scrvica · sLLE ANALYSES REQUEST•:· Staie ubora-, of Public: Health
P. 0. Box 28047
306 N. Wi1mffll'I'!"' Street
l\alcigb,276ll
:Number :J'fdJl:ZZ:Z.C.Jtf-ZS" J 'ic? Fid4~1!)PkH~ -. .. . ..... .
:neofSi~ CJ,~n,,,e/ .ct?,, cf~r: , -·Sir.Loc:a:iou-t7i~.,.o,/J At1C:c-=·
llectedBy J:.dl«t"/c,,,, · IDlf__._7'_5£.,___· __ DateCollccred 7-Jo':..\f7 ...... Time //,'00
;:-. of Sample:
~nvironmental
-Groundwater ( 1).
-Surface Water (2)
✓ Soil (3)
-Other (4)
Concenttate
__ Solid (5)
--liquid (6)
__ Sludge (7)
--Om~ (8)
Comments
z_F
INORGANIC CHEMISTRY ''i~;.
Extractables Tora!,.
Parameter
-Arsenic
_Barium
-Cadmium··
-· Chromium.
-Lead
_Mercury
-~J~t1il!!,D __
-·Silver
Results mg/1 Parameter
_Anen&:
.:..__ Barium ·
-,------· -.Cadmium.
.:..__ Chloride .
_Chromium
_.Coppet
_Fluoride·
_Iron
_Lead .. ·:, .. •:,'
---•-•::_~·-__ ·,_=-!_• .. · .... ~-·---· -~--_Mangrnere--.
_Mercury
_Nitrate.
_Selenium
Resulll nig/1 Jji Parameter
· ,,.;;ll4 · Silver ' :·· , · ------·-" ______ ..::i;_Sulfata .. ,., •
~Zinc -___________ , ·~Pb
',,_ 2'.=Conductivity
.;:;_;_ms
----,----_;;.;_TOC
Resulamg/1
ORGANIC CHEMISTRY
Parameter
_ P&. T:GC/MS
L Acid:B/N Ext.
_TOX
Parameter
Reauhsmg/1
MICROBIOLOGY
_ (MF) Coliform Colonies/lOOmls
_ (MPN) Coliform Colonics/lOOmls
)ate Received 7-3 /-f1 'Vi p
. 511/t. ·[)
)ate Extracted ~-/ I-17] /./
Paramecer·
-EDB
-PCB•s··.
_Petroleum
_Endrin
_J;ndane
______ . :__Methoxychlor
______ ~ Toxaphenc
---------:__2,4-D
Results mg/1
________ 2,4,S..TP (ailva) _____ _,
Parameter
_ Gross Alpha
_GrossBcm
RADIOCHEMISTRY
ResulaPCi/1
Date Rcpottcd -;;:72r-;--------------
Date Analy:cd tJ.N/.1,i-J-7 L,,J)
.e;,orted Bv ---------------Lab Number 7Q2015
C:Depa~ 0(l!,,mar1 Resourca
·is ion_ of Healµ, Scrvlca dtn,LE ~ALYSES REQUEST. Stau: Labontory of Pubiic Hdt'.·,
P.O. Box 2BC47
306 N. WWllington St=t
llaleigh, 27611
:Numbtt :Jo/t/)12.2:Z.C.]JJ-ZS" Fid4~~~,.;;;L;,,;. r .... -=c...,7.==-=-=-=-..,.· --------
me of Si~ · C,1, Q n "'"" I d&r cf e; · --Sir~ ~01'.l • &7 c::I 71·~v1J kt Cr,· ---
llected By J:.,ll«tlc,,,, ID#___._?:_;,:_· __ DateColleaed 7-JO-J-7 Time /2,'0c>
;,c of Sample:
:'.nvironmental
-Groundwatct (1).
-Surface Water (2).
✓ Soil (3)
--Other (4)
Concentrate
--Solid (5)
--Liquid (6)
__ Sludge n>
__ C)mc:r (8)
Comments
· · --•-;,c•· INORGANIC CHEMISTRY
Parameter
-Arsenic -·.
-·Barium _-·----·:-: ..
_ Cadmium',.· :
_ . Chromi1.mt;. · ·
-I.cad .,.:,:;~T-.' ·
_ Merc:ury:''·ii.'." ·
-~J~"!il!!ll -:.: .
_-Silver
Parameter
·_Arsenic
;__Barium'
-------•-Cadmium..
__ • ·-: ...... "7· .... -::-_• ____ ~Chloride-.
_Chromium
_.Copper
_Ruoride·
_hon
;__Lead,•:-.,..:.:.
-___ ._ .. , .. _:'! .... "·-__ -.... ::'::"_y:'._.·.:·------·~ ·,-·_Manp:i:e;re--
_Mercury
_Nitrate,
_Sdenium . _. ':'\ ...
Total
Resulamg/1 Parameter Results mg/1
______ . __ Silver
________ sulfates -·
_Zinc _
-------__ Pb
__ Conductivity
_ms _. _Toe
ORGANIC CHEMISTRY
Parameter Remlami/1 Parameter'
_EDB-·
_PCB•s--. -P&.T:GC/MS
L Acid:B/N Ext.
_TQX ______ . _Petroleum
MICROBIOLOGY
P~eter
_. (MF) Coliform Colonies/lOOmls
_ (MPN) Coliform Colonies/lOOmls
>ate Received 7 -3/-<ff 71( P
. ~µ{/ -
>ate Extracted 'j,JJ•Y?l.!Jf).
_ Endrin
_l.indane
· Parameter
______ . --Methoxychlor
_______ Toxaphene
-2,4-D
Results mg/1
-2,4,5-TP(silvcx) _____ _
Parameter
_ Gross Alpha
-Gross Beta
RADIOCHEMISTRY
Results PCi/1
Date Reported -::--:-;;r.-------------
Date AnaJvied _f6_JJ.__,~'--,_l 7,_::::t_,,__.7__.8_...;J);;:;.· ______ _
~;,orred By ______________ ub Number _ __.7_.0a<-.:2=0_1...;6;;;.._ ____ -,. __ _
•.'-!< ,tcll /R..,...d 7/851
DIVISION OF HEALTH SERVICC:S
SOL~ HAZARDOUS \/ASTE MANAGD£KT .CH
Chain of Custody. Record
Hazardous \laste Materials
Location of Sampling: Generator __ Transporter _Treatment Facili1
__ Storage Facility __ Disposal Facility _Landfill
✓ Other: C/eq,.~
Company's Name C 4a y,,-,e,/ /10ts7'--e·v Telephone( 'fl'T) b r :J-y £7' 0
Address O ,x -;r;,,.q/. /1/>C; 7 .
Collector's Name ~/
7_~ signature
Date SampledG)??:#Jq, 17'.cf'Z Time Sampled //-/,7../00
Type of Process Generating \laste &.rq/ //q,--/✓-.nt¥' S/4✓q·e--• ·--=--'="--'=----"'---='-'-~_./~'----'--""--:CC_✓'-7"-='-------
. Field Information
Field Sample No. Jo t5 r-J 6 & 6 3 6 C7
Chain of Possession:
7-3 0-t-J 1-?7
inclusive dates
title inclusive dates
3.
signature title inclusive dates
Results reported
signature ti~le date
Instructions: Complete all applicable information incl~cing signatures, and submit with·2nalysis request forms.
BASE/NEUTRAL AND ACID
EXTRACTABLES
C01PWND
• • STATE LABORATORY Of PUBLIC HEALTH
DIVISION DF HEALTH SERVICES, N.C. DEPARTPIENT Of HUMAN RESOURCES
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGAN C CHEMICAL Al LYSIS
LAB NO 7t.n n/U (.)/~-<'70?/1/ ,t,
FIELD# .:J/-G tr' 3&,£~ ~/.C 7
TYPE I :?l ( ~) ( 3 l ( \ ( l ( l
UNITS ••n/1,<.;;/kn' ua/1 ,i 1'/l«i un/1 ./4/kn un/J ••n/kn .,n,J un/kq ua/1 un/ka
N-nitrosodimethvlamine ·-1 (/) ,7 r • /A
' bi s(2-chloroethv1 )ether
2-ch 1 o~heno 1
ohenol
1 3-dichlorobenzene
1.4-dichlorobenzene
1 2-dichlorobenzene
bis(2-chloroi llether
hexachloroethane
N-nitroso-di-n lamine
nitrobenzene I
i snnhorone
2 nit~henol
2. 4-dimethvl oheno 1
bisf2-chloroethoxvlmethane
2.4-dichloroohenol
1.2.4-trichlorobenzene
n.,nhtha 1 ene
hexachlorobutadiene
4-chloro-&-Cresol
hexachlorocvcl~ntadiene
2.4.6-trichloroohenol
2-chloron>nhthalene
acen•nhthvlene
dimethvl ohthalate
2.6-dinitrotoluene . I
acen•nhthene
2.4-dinit~henol .. 1/..tJO
2 4-dinitrotoluene ?1~0
4-nit~henol J u,o
fluorene ~o
4-chlo~henvlnhenvlether '!JD
diethvl ohthalate ·. ,, ti
4,6-dinitro-o-cresol J" {70
diohenvlamine .&,00
azobenzene I (10
4-bN"nVV>henvlohenvlether ,~O
hexachlorobenzene . 2,J
nontachlo~henol 1,;, ,t:JO
ohenanthrene 'Cl30
anthracene 3 '>O
dibutvl ohthalate 330 . I I
fl uoranthene '3 ·io \ ' I \
m~
J -Estimated value. JA-lr/for-K -Actual value is known to tk fess t~an value given. L -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. The numer is the Mini"""' Detection Limit. =~./:)"-
NA -Not analyzed. 1/ -Tentative identification.
~I -On NRIJC List of Priority Pollutants.
N. C. Viv.u.,ian 06 He.a.Uh Sv,_vic.e./2
VHS 3068-0 (4/86 Laba~a;to~y)
BASE/NEUTRAL ANO ACID
EXTRACTABLES
OOIWOUNO
nvrene
benzidine
butvl benzvl ohthalate
benzlalanthracene
chrvsene
3 3-dichlorobenzidine
bis(2--ethvlhexvllnhthalate
di-n--octvl ohthalate
benzo(blfluoranthene
benzolklfluoranthene
benzo(a)nvrene
indenoll 2 3-cdlnvrene
dibenzo(a.h)anthracene
benzoln h il=rvlene
aniline
benzoic acid
benzvl alcohol
4-chloroaniline
di benzofuran
2--methvl=nhthalene
2--methvlohenol
4--methvlohenol
2-nitroaniline
3-nitroaniline
4-nitroaniline
2 4.5 trichloroohenol
J -Estimated value.
• •
STATE LABORATORY Of PUBLIC HEALTH
DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES
P.O. BOX 28041 -306 N. WILMINGTON, ST., RALEIGH, N.C. 21611
ORGANIC Q-IEMICAL ANALYSIS
LAB NO -Jf)::J/1/U 7l>;2.o/~ 7D2-af/_
FIELD# ~/4 & ~ ... ,. I,; ,,, ·-11.,-:; /
TYPE (""", ( . l ( '.3 l ( )
UNITS un/ 1 ,<, n/kn un/1 n/kn un/~ uo/ko .. n/1 ,,n/ka
---~ 0 r. :; -r 7A
/1. (;"0
_: 3V
-::r·~v
; -~{}
/t,(),P ·_,.,f b
:-, ~t-'
;r;, o<J
, . I/ ,
V \'
/{;(Ir.I /~ /., I
IL,t>CI 'I
;,Flt)
/ .
Jt,(i Cl
I , I
' I \V \I/
r ,, /Ji-
,, ,:,./ i,,; .
I f' '
K -Actual value ls known to be less than value given.
( ) ( l
""/1 ""/kn un/1 .. n/ka
L -Actual value is known to be greater than value given.
U -l\aterial was analyzed for but not detected. The nurt>er is the Minirrun Detection Limit. =--ml),t__ · NA -Not •nalyzed. I/ -Tentative identification.
~I -On NROC List of Priority Pollutants.
N. C. D-<.v-U-<.on o 6 Ilea.Uh Sviv-<.c<v.,
DHS 3068-0 (4/86 Labo1I.a.to~y)
•
October 7, 1987
TO: File
FROM: Mary Giguere ('f,.0
RE: Site U.S. 1 to Channel Master NCD 122163825
On October 12, 1987 Jack Butler and Stan Atwood will b_e,. going to the
Channel Master Site to observe a sludge drying process and i:o split samples
with the company. The samples will be of soil that is comprised of clean fill dirt. The samples will be taken by Channel Master and given to Jack Butler.
This site can be visited in Level D protection
MG/pb/0489b.10
• •
02 October 1987
To: File
From: Jack Butler
Subject: Channel Master, NCD122263825
Doug Holyfield, NC DHR/DHS, was updated on the status of the
cleanup activity at the subject site on 01 October 1987. At Mr. Holyfields
request, Larry Perry, NC DHR/DHS, was contacted on 02 October 1987 to discuss
this site. Mr. Perry reported that he visited the site a couple of weeks ago
and thought that the cleanup was going well. Mr. Perry was informed that the
NC CERCLA Unit was planning to be at the site on 09 October 1987 to split soil
samples from the bottom of the excavated lagoon area.
JB/ds/0469b.41
•
To:
From:
Subject:
• •
02 October 1987
File
Jack Butler
Telephone conversation with Roger Coats [phone] conceraing
Channel Master, NCD122263825
Mr. Coats was contacted on this date to reschedule our sampling
visit for October 9 to October 12, 1987.
JB/ds/0479b.40
'.
,
To:
From:
subject:
• •
01 October 1987
Pile·
Jack Butler
Telephone conversation with Roger Coats, Channel Master [phone], about sampling soil in bottom of lagoon
on Channel Master Site, NCD122263825
Mr. Coats contacted our office on this date to discuss sampling of the. lagoon sub-soils on the subject site, A date of 09 October 1987 was set for sampling 2 of the 4 quadrants of the soil under the lagoon, a lagoon inlet point, and 2 background points, Samples will be collected at 0-3 inches and 12 inches depth for a total of 10 samples. Samples from each of the 2 quadrants will be composites of 5 points in each quadrant, Sampling will ·be conducted by an independent contractor and will be split with the NC CERCLA unit, The CERCLA samples will be analyzed for both inorganics and organics including total cyanide, Mr. Coats elected to have the Channel Master samples analyzed for the same constituants despite the fact that the cleanup plan only calls for analysis for metais. and total cyanide,
JB/ds/0479b/42·
To:
From:
Subject:
• •
01 October 1987
File
Jack Butler
Telephone conversation with Roger Coats, Channel Master
[phone], about sampling soil in bottom of lagoon
on Channel Master Site, NCD122263825
Mr, Coats contacted our office on this date to discuss sampling of
the lagoon sub-soils on the subject site. A date of 09 October 1987 was set
for sampling 2 of the 4 quadrants of the soil under the lagoon, a lagoon inlet
point, and 2 background points, Samples will be collected at 0-3 inches and
12 inches depth for a total of 10 samples. samples from each of the 2
quadrants will be composites of 5 points in each quadrant. Sampling will be
conducted by an independent contractor and will be split with the NC CERCLA
Unit, The CERCLA samples will be analyzed for both inorganics and organics
including total cyanide. Mr. Coats elected to have the Channel Master samples
analyzed for the same constituants despite the fact that the cleanup plan only
calls for analysis for metals and total cyanide.
JB/ds/0479b/42
• Date
ROUTING AND TRANSMI LIP/ ?1"
TO: (Name, office symbol, room number.
b
1.
2.
3.
4.
5.
Action
Approval
AIJ Requested
Circulate
Comment
Coordination
FIie
For Clearance
For Correction
or Your lnfonnatlon
Investigate
Justify
Initials Date
Not& end Return
Per Conversation
Prepare Reply
See Me
Sigfl&ture
~-~-~~ /P~~.
· .. 0 ' ~~ e, ~~ 44 ~$R/. . .
00 NOT use this form as a RECORD of approvals, concurrence·s, disposals, · clearances, and similar actions ·
FROM: (Name, org. symbol, Agency/Post)
. '
,;t-!D-S FG
OCT C
Roger Coats
Channel Master, Di vision of .Z\vr/~:::.._.
P.O. Box 1416
Industrial Park Dr.
Smithfield, North CaroJ.ina 27'.:·.:7
Dear Mr. Coats:
This letter is written to acknoi:ledge ci"il' s :-eceipt of the Cl_eanup
Plan submitted by your office £er-the C:-.arinel :·!aster: Site, located. in
Oxford, North Carolina.·. .-.-(\1t.-:
~~ ., -. -,':;-.;-.,: :1:.
Ei'A has no comment at this point rn_tfr,-.. e;r.corrmunication_.with.Jac(Butler ..
of Nortf1 .Carolina Division ·of Haalth,Services, .CERCU:1:uni't}'has>assurec!\ :-
EPA that:.· the State of· North:'caroli'na/ is viorkirig ·closelv\11th1:yoti'F' people · ·
and' that the work' has ·prog'i~ssed s,::;ffsL1ctori1·,::'1
• -,. ·:_ :. '.'>Vt('· • ,-; <' .. ; .'.
: . -, .:.-:a, ). . . ~-,:' ·. •:'•". :·:.'· '.:.~(<·: ·, \,\J\J ;~{·:.:' ,'. .. -._ .. , .-+~···_;;;,-~;;~-~;:{.'.:>' >:• J.
Please be'aware,'howeve:-, of th-2 status of tl1e.Channel 11aster Site within
EPA. ; The, site hak been subjeclced fo ti,,3. I·laza:-d Ranking System (HRS) and·
b .. l ded . th. N t' l p'••, ·,1.-~ . L" · rr-,pr• ·-sh 'd th .. ,·<-:1:~i{;·•·-·;·may.,. _§?,~:-lnc ...,_u pn:\f ... ~1...,1 a 1ona .. r:10:r:~_L.o.8~~. ~S~·..-\._,. L) .• ,.1,_,._ .iQU.~ .... }-.s ... occ~1_
·. full Site charact~rization and ~ppr_opriaC:e cleanup ivili' I-~,-~<:requl~eo· under.
CERCLA in order t_o delete tl:e ,,,site, tr-om the NPL; ·. · · · '·
Please feel free to contact me
regarding th.is matter.
Sincerely, 1a·
_·, f /)
,, ,.~ "'-~ ✓ ,.__)(Ji{!tl:. /---/da 1\{J!'-'l--f(_j:1c!',~1
Barbara Hansen Benoy (;
Environmental Scientist
cc: Felicia Barnett
,Jack Butler
,: -,,.
(404:, 347-3402 if you have any questtons
• •
September 15, 1987
TO: File
FROM: Mary Giguere~ G.
RE: Site U.S. 1 to Channel Master NCD 122263825
On September 16, 1987, Jack Butler Cheryl McMorris, Grover Nicholson,
and Pat DeRosa will be going to the Channel Master Site to observe a sludge drying process and to split samples with the company. The samples will be of soil that is comprised of clean fill dirt. The samples will be taken by Channel Master and given to Jack Butler. This site can be visited in Level D protection.
MG/pb/0489b.9
• •
August 24, 1987
TO: File
FROM: Mary Giguere ~6
RE: Site U.S. 1 to Channel Master NCD 122263825
on August 25, 1987 Jack Butler, Stan Atwp9d and Mark Durway will be going to the Channel Master site to observe a sludge drying process and to split samples with the company. The samples will be of soil that is comprised of clean fill dirt. The samples will be taken by Channel Master and given to Jack Butler. This site can be visited in Level D protection.
MG/pb/0489b.8
....