NCD122263825_19850925_JFD Electronics - Channel Master_FRBCERCLA SPD_Groundwater Monitoring-OCR

• SOIL & MATERIAL ENGINEERS, INC. ENGINEERING-TESTING-INSPECTION
1903 Harrison Avenue, Box 609, Cary, NC 27511, Phone [phone]
. September 2.5, 198.5
North Carolina Department of Natural Resources
and Community Development
Division of Environmental Management
P.O. Box 27687
Raleigh, North Carolina 27611-7687
A ttentlon: Mr. Edward L. Berry
Reference: Permanent Ground Water Monitor Wells
Channel Master Satellite System, Inc.
Oxford, North Carolina
S&ME Job No. 0.5.5-8.5-139-A
Gentlemen:
~
GROUND WATER SECTION
RALEIGH, N. C.
Soil & Material Engineers, Inc. has been authorized to install four to five
• permanent ground water monitor wells at the Channel Master Satellite System, Inc.
facility, The wells are being installed around a lagoon used by a previous owner to hold
chromium waste sludge.
The monitor wells will be constructed to the standards discussed in 1.5NCAC
2C.0J08, Standards of Construction: Wells other than Water Supply (C). Upon
completion, Soll & Material Engineers, Inc. will complete Well Construction Record Form
GW-1 Revised 11/84 and submit them to the Division of Environmental Management.
Enclosed Is a completed Application for Permit to Construct a Well Form GW-22,
If there are any questions concerning this request, please contact me at 481-0397,
Sincerely yours,
BDT/sws
Attachment
SOIL & MATERIAL ENGINEERS, INC,
.:b~~I~
Senior Hydrogeologist
RALEIGH, GREENSBORO. ASHEVILLE. WILMINGTON, FAYETTEVILLE, CHARLOTTE, NC SPARTANBURG, COLUMBIA, CHARLESTON, MYRTLE BEACH, GREENVILLE, SC · ATLANTA, ALBANY, ST. MARYS. GA-TRl·CITIES. TN-CINCINNATI, OH-f'r . "01.D BEACH, ORLANDO, TAMPA, FL
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NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF NATURAL AND ECONOMIC RESOURCES
APPLICATION FOR PERMIT TO CONSTRUCT A WELL CM-1 through CM-5
To: NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION 24 Sept. 198,
Gentlemen:
In accordance with the provision of Article 71 Chapter 871 General Statues of North Carolina, and regulations pursuant thereto, application ls hereby made by Channel Master Satl!!Jllte Systems, Inc. for a permit to construct a well as described below and In the accompanying data submitted as a part of this application. (a) Name of Property Ownen Channel Master Satellite Systems, Inc.
(b) Location of Property: Industry Drive Oxford Granvllle
(Road, Community, Subdivision, Lot No.) Town County
(C)
(d)
Purpose of well: Monitoring .
Will proposed well replace an existing well:
(e) Total capacity of existing system: N/A
Well No. Yield
No
Well No.
• (f)Proposed wdl:
•
Construction type: Screened (open end, screened, gravel packed, etc)
Estimated depth: 20 to 30 feet Estimated Yleld:_,N_./ .... A ____ _
Estimated date of construction: Begin 26 September 8, Complete 28 Sept 8'
(g) Drilling Contracton SclcME Drilling, 0412
(h) Location of Well: Provide a detailed map showing the location of the proposed well and any wells in the existing system to at least two (2) nearby reference points such as roads, Intersections, and streams, Identify roads with State Highway road identification numbers. Show all existing water supply wells within a radius of 1,000 feet of the proposed well.
(i) Well Construction Diagram: Provide a diagram showing proposed construction specification. (See Form GW-22A)
The Applicant hereby agrees the
proposed well will be constructed in
accordance with approved specifications
and conditions of the Well Construction
Permit. --
Senior H ydrogeologlst
Title
gent
Soil clc Material Engineers, Inc.
P.O. Box 609; Cary, NC 27.511
(Malling Address of Agent)
PERMIT NO, Issued 19 ---

-
-
-
--
Stralght-SCreened
or
Gravel-Packed Well
DUGR.\.'l Ill-' 1,101'0:iEn
CCMT!lllCTIOS Sll:ClflCATlOHS
Oron-Ead Woll
.(Con,tructed la uaco~aolldated lorution1) .. ' " .
, .( c~n• true t.ed 1 a conn 11 d-
• ted lo~ationa)
•
•
land 1urlac•---------...
A) Ce~f/-
l)• ll\llar, Ne t -•" I 1Pe_"'<C _____ I. D, ___ lba, ft, d..,--f· .. :;,· ·: ,i;
~ -2)_.,. fvL t
· {depth) · _ft, (iDto rock)
ype .:J." I. D,. lba,/ft,
. ~D f.t. (depth) .,.. /, S° ff.
B) Ce■•:l'.J~
1) ~ &',harr
. 2) Cellar:
i .
I C) Screea(a), eve.
i i ~-i rJ.4//,w /.lS"
.3R cit> "• fJ"'"'' ✓N/' p 0 ..
ft, to --:(J:;;,___,;I t •
ft, to tJ .ft,"'·•m-r.,n.rr.'ffl1'1'1,.rl .....;:;..... __ . Rock '
_t1J)O z_ 1~ __ 1, D,
.... r.t. to ,J.s ___ .ft.
_ft. to 'p2o ft •
I) , D) GraYol: /!.~ 0 . p ,,
"-6
}, L,... •t. to ~,. __ ._ft, ___ _,,in.
(ahe) , , (Fill in each 'blank that applies and uao appropriate dia1raa o-to ahov propoaed coaatru
II' ~ caainc (outer and iuner) , -'• etc.) 1 packer■, ■creeu, ~
ct.ion including, but not liaited to, , aeolinc aateriel (cuaent, cla7, rravel, chemical feed line•, etc,)
Locatioa·DlegTaar (PreYiou1l7·prepared ■-p~ u7 be 1u'b■ltted provided tbe7 co-
t.in information req~lred in ite■ (r) ol the application),
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SOIL & MATERIAL ENGINEERS INC. ENGINEERING-TESTING-INSPECTION
1903 Harrison Avenue, Box 609, Cary; NC 27511, Phone [phone]
March 24, 1986
North Carolina Department of Natural Resources and Community Development
Divislon of Environmental Management
P.O. Box 27687
Raleigh, North Carolina 27611-7687
Attention: Mr. Edward L. Berry
Reference: Permanent Ground Water Monitor Wells
Channel Master Satellite System, Inc.
Oxford, North Carolina
S&:ME Job No. 05.5-85-139-B
Gentlemen:
• Soil &: Material Engineers, Inc. has installed five permanent ground water monitor
wells at the Channel Master Satellite System, Inc. facility. The wells were installed
around and through a lagoon used by a previous owner to hold chrom.ium waste sludge.
The monitor wells were constructed to the standards discussed in l5NCAC
2C.0J08, Standards of Construction: Wells other than Water Supply (C). Enclosed are the
well completion forms for the state of North Carolina. The mailing address for Channel
Master Satellite Systems, Inc. is:
•
P.O.Box 1416
Smithfield, North Carolina 27 577
Attn: Mr. F ellx Killette
If there are any questions please contact me.
· S Ince rely yours,
SOIL &: MATERIAL ENGINEERS, INC.
~5~~~~
Bryson D. Trexler, Jr., Ph.D., P.G. Senior Hydrogeologist
i,OT/sws
RALEIGH, GREENSBORO, ASHEVILLE. WILMINGTON, FAYETTEVILLE, CHARLOTTE, NC STARTANBURG, COLUMBIA, CHARLESTON, MYRTLE BEACH, GREENVILLE, SC ATI ANTA Al RANY C:::T UAOYC! ~" Tn1 r-1T1r-r Tu ,..,,.,,...,.,.,._, -·· ----·--
IIORTM CAA(\N DEPARTMENT Of NA T1JIIAI. RESOUICES AHO COINJNITY DEVELOPMEHT DMSIOi.; Of ENVlRONl,EHTAL MAHAOEloENT • OROI.N)WATSI SECTION FOR OFFICE USE ONLY
P.O. IOX 27917 • IWBQH,K.C. 27111, PltOIE (111) 7i3·IOl3 Quad. No. ______ Serlal No. __ _ Lat. ______ Long. ____ Pc_
• WELL CO~STRUCTION RECORD MW-1
(c,-,)
Minor Buln ___________ _
Baaln Code ___________ _
Header Ent, ______ GW-1 Ent.-
)RILLING CONTRACTOR Soil & Material Drilling Co,
)RILLER REGISTRATION NUMBER __ ......c4.:..:1:..:2,_ ___ _
WELL LOCATION: (Show skelch of the location below)
Nearest Town: _.::_Ox::.f:.o::;r::.;d=---------------
Industry Drive
(Road. Community, or Subdivision and Lot No.)
OWNER Channel Master Satellite Systems, Inc.
ADDRESS~P~·~Pu•~»xoax_1~4u1~6'-r.,.,.--,-~--,,......-------
(Streel or Roule No.) Smithfield NC 27577
City or Town , Slate Zip Code
DATE DRILLED 9-26-85 use OF WELL Monitor
TOTAL DEPTH 15 1 CUTTINGS COLLECTED O Yes O No
DOES WELL REPLACE EXISTING WELL? 0 Yes ~ No
STATIC WATER LEVEL: ____ FT. □ above TOP OF CASING, D below TOP OF CASING IS 1.5 FT. ABOVE LAND SURFACE.
YIELD (gpm): _____ METHOD OF TEST ______ _
WA.ZONES (depth): ______________ _
:HLORINA TION: Type ____ _ Amount ______ _
CASING:
Depth Wall Thickness Diameler or Weight/Fi, Material
From 3,5 To -1,5 Ft. 2" a. 154
From To Ft.
From To Ft.
:lROUT:
Depth Material
From _o~_To 1.5 Ft. Portland
Method
Poured
From 1.5 To 3.0 Ft. l" Bentonite Pellets
SCREEN:
Depth Diameter Slot Size Malarial
From 13.5 To3.5 Ft. in.Q Q]Sin. P)lC
T F . . ~ <jD fr~m ____ o ___ t. ___ .,_ ___ ,n.
From ____ To ___ Ft. ___ in. ___ ln.
)RAVEL PACK:
Depth Size Material
.m 15.0' To 3.0' Ft._a.aM.._or .. t.,a,..r~-Quartz rrom ____ To ___ Ft _____ _
STATE WELL CONSTRUCTION PERMIT NUMBER: 38-0100-WM-0012
County:
Depth
From
o.o
6,0
8,5
11.0
14.0
Granville·
To
~.Q
8.5
11.0
14,0
15.0
DRILLING LOG
F orma tlon Description Tan to Brown Clayey sn,T
Brown Silty CLAY
Tan Brown Clayey SILT
Brown Silty Fine Sandy CLAY
Sand, Tan to Brown Clayey Silty
Coarse SAND
II additional space is needed use back of form,
LOCATION SKETCH
(Show direction and dislance from at least two State Roads, or other map reference points)
..
tEMARKS: ------------------------------------------
1 DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15 NCAC 2C. WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS REC~4.,;;;5'.6;;;~0,~ WELL OWNER. . ::?&lft
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NORTH CIJIOl.lHA DEPAAn.ENT OF NATUW. AEIIOUICU AHO COl,MHTY DEVELOPMENT FOR OFFICE USE ONLY ' . Ct~ON OF ENVI-AL MANACIDEN'T -CIROUNlWATEJI SECTION
. P.(I. IOX 27087 -AALEIOH,N.C. 27111, PH0N! (818) 7:13-&0N Quad. No. ______ Serial No. __ _
Lat. ______ Long. ___ Pc_ Minor Baaln ___________ _
WELL CO~STRUCTION RECORD • MW-2
(c1.1-2.)
Basin Code ___________ _
Header Ent, ______ GW-1 EnL_
DRILLING CONTRACTOR _S:;.;o:..:i:.::l_&;_::,Ma:::..:;te:.:r:..:i:.::a::.l :..:D:..:r..=i::.ll::.:i:::n:Ji!g_C:;.;o:;.;•:....
DRILLER REGISTRATION NUMBER __ 4_12 ______ _
. WELL LOCATION: (Show sketch ol Iha location below)
Nearest Town: ___ O_x_f_or_d ____________ _
Industry Drfve
(Road, Communily, or· Subdivision and Loi No.)
. OWNER Channel Master Satellite Systems, Inc.
ADDRESS P.O. box 1416
(Street or Route No.) Smithfield NC 27577
City or Town
DATE DRILLED __ 9_-2_6_-_8.;,.5_
State Zip Code
USE OF WELL __ M_o_n_i_t_o_r __
. TOTAL DEPTH _.,:1.:.5~.0,.___ CUTTINGS COLLECTED }O!) Yes O No
'DOES WELL REPLACE EXISTING WELL? □ Yes @.:No
. STATIC WATER LEVEL: 7.85 FT. 0 above TOP OF CASING, D below TOP OF CASING IS _ _.,J.,_, .,__5 _FT.ABOVE LANO SURFACE .
. YIELD (gpm): _____ METHOD OF TEST ______ _
. W-R ZONES (depth):
---------------CHLO R _IN A TION: Type ____ _ Amount
I. CASING:
Wall Thickness Material
PVC
~~ilo
Depth Diameter or Weight/Ft.
F 3.5 T -1 5 211 0,154 rom __;;;.:..;::__ o • Ft. __ _
From ____ To ___ Ft .. __ _
From To Ft.---
. GROUT:
Depth Material Method
From Q To 1.~ Ft. :f~n;:tlansi PQYI!ld
From 1,5 To 3.0 Ft Bentonite ·seal
. SCREEN:
Depth Diameter Slot Size Material
From 13 5 To 3 s FI. in. 0,05 in. -!x:ti
f1Jm To Fl. In, in.
From To Fl. in. In.
GRAVEL PACK:
Deplh Size Malarial
.om 15.0 To 3.Q Ft. Mortar Quartz Sand
rom To Ft.
REMARKS:
STATE WELL CONSTRUCTION
PERMIT NUMBER: ____ ..:3c.::8_-0::;,al:..::0:.:0_-WM==---=0.=.0:.:l 2:__
County: Granville
Depth DRILLING LOG
From To Formation Dt/crtpdog o.o 9.0 Brown to Orange ine and:x Sil
CLAY
9.0 11.0 Gre:x to Green Plastic CLAY wit
Organic Matter
11.0 14.0 Green to Brown Sil t;r Fine Sand·
~LAY
14 .o 15.0 Red to Orange Clax!ll SiH:t Fyj•
to Coarse SAND
II additional space is needed use back ol form.
LOCATION SKETCH
(Show direction and distance lrom at least two State Roads. or 01her mao reference ooints)
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Channel Master Satellite Systems, Inc. Oxford, North Carolina
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~ . NOii'!!,~~ DEPARTMENT OF NAt\JIW. RESOIJICES ANO CCMIJNTY DEYEI.OPleff . • 0MSIOH OF ENVIAON,ENTAL MANAGEMENT • CIAOIN)WATER SECTION FOR OFFICE US£ ONLY
•
,.o. eox a1ee1 • RALEIQH.H.C. 21111, -1t111 7~·eol3
WELL CO~STRUCTION RECORD MW-3
(c~-~)
DRILLING CONTRACTOR Soil & Material Drilling Co,
DRILLER REGISTRATION NUMBER ~--...:..4;;;..;12::_. ___ _
I. WELL LOCATION: (Show sketch of lhd location below)
Nearest Town: __ O_x_fo_r_d _____________ _
Industry Drive
(Road, Community, or Subdivision and Loi No.)
2. OWNER Channel Master Satellite Systems, Inc.
ADDRESS P.O. Box 1416
(Street or Roule No.} Smithfield NC 27577
City or Town • Slate Zip Code
I. DATE DRILLED 9-26-85 USE OF WELL Monitor
I. TOTAL DEPTH __ 1_5_. O __ CUTTINGS COLLECTED J@ Yes
i. DOES WELL REPLACE EXISTING WELL? 0 Yes Jl!Kl No .
i. STATIC WATER LEVEL: 7.85 FT. 0 above TOP OF CASING, D below TOP OF CASING IS __ l_._5 __ FT. ABOVE LAND SURFACE.
'. YIELD (gpm): _____ METHOD OF TEST ______ _ . W. ZONES (daplh): ______________ _
. CHLORINATION: Type ____ _ Amount
I. CASING:
From
From
From
. GROUT:
From
From
SCREEN:
From
fr.>m
From
Wall Thickness Deplh Diameter or we,ghl/Ft. Malarial
_3~·~5~To -l.SF1. 2" 0.154 PVC
'S...~ 40 ---TO ___ F1. __ _
---To Fi.---
Depth Material Method
Poured 0 To l. 5 Ft. Portland ---___ To ___ Ft. _____ _
Depth
13,S To 3 s Ft.
To Ft.
To Ft.
Diameter
in.
in.
In.
Slot Size Material
a as ,n. yvc ~(1/0 ___ ,n. ---
___ in.
GRAVEL PACK:
Depth
.• om. 15.0 To
From To
REMARKS:
3.0 Ft.
Fl.
Size
Mortar
Material
Quartz Sand
Quad. No. ______ Serial No. I Lat. ______ Long. ____ Pc_ Minor Basin ___________ _ Basin Code ___________ _ Header Ent, ______ GW-1 Ent. __ _
STATE WELL CONSTRUCTION PERMIT NUMBER: 38-0100-WM-0012
County:
Depth
Fr,;im u.o
5.5
10.5
14.0
Granville
10.5
14.0
15.0
DRILLING LOG
Brown sf ~'tya'~rJ!scrlption
Grey Slightly Silty Plastic .CLA'.
Grey to Green Slightly Sandy
Silty CLAY
Orange to Brown Silty Coarse
to Fine SAND
If additional space is needed use back of lonm.
LOCATION SKETCH (Show direction and distance from al least two Stale Roads. or 01her map retere_nce points)
I DO HEREBY CERTIFY THAT THIS WELL WAS CD STRUCTED l~C~ANCE .WITH 15 NCAC 2C. WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RECORD AS BEEN ~EDT ~ WELL OWNER. II . . lv ~ h~ . _') r;..,,. A • I/ P'I
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Existing Building
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Channel Master Satellite Systems, Inc.
Oxford, North Carolina
• •
-TII CAR()l,JNA DEPARTl.ENT OF NA nJAAL AESOUICES ANO COIMHlY DEVB.OPMEHT
OIVISla. OF ENVIAONl,£NTAL MANAGEMENT -OA0UClWATER SECTION FOR OFFICE USE ONLY.
P:o. eox 21ea1 -AAI.BOH.N.C. 21111, PHONE [phone]-eoa., Quad. No. ______ Serial No. __ _
Lat. Long. ______ Pc_
• WELL CONSTRUCTION RECORD (~~L/)
Minor Baaln ___________ _
Basin Code ___________ _
Header Ent, ______ GW-1 Ent._
DRILLING CONTRACTOR Soil & Material Drilling Co.
DRILLER REGISTRATION NUMBER __ 4 __ 1_2_· ____ _
. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Oxford ---'===--------------Industry Drive
(Road. Community. or Subdivision and Lot No.)
OWNER Channel Master Satellite Systems, Ioc,
ADDRESS P. o. Box 1416
Smithfield (Street or Rowe No.J 27577
City or Town Slate Zip Code
DATE DRILLED 9-26-85 • USE OF WELL Monitor
TOTAL DEPTH 15,0 CUTTINGS COLLECTED XXYes O No
DOES WELL REPLACE EXISTING WELL? 0 Yes :E;a No
STATIC WATER LEVEL: __ 7_,8_5_ FT. 0 above TOP OF CASING. D below TOP OF CASING IS _...;1:..;•:..:5::...-_FT. ABOVE LAND SURFACE.
YIELD (gpm): -----METHOD OF TEST ______ _
W.11 ZONES (depth): ..;.... _____________ _
CHLORINATION: Type ____ _ Amount
•. CASING:
Depth Wall Thickness Diameter or Weight/Ft. Material
From ___.3.._.5_ To -1. 5 Fl. 2" 0 .154 PVC xJ_ qo From ---TO ___ Ft, __ _
From To Fl.---
. GROUT:
Depth Material Melhod
From 0 To 1. 5 Ft. Portland Poured
From 1.5 To 3.0 Fl. Bentonite Seal
. SCREEN:
Depth Diameter Slot Size Material
From 13,S To J,S Ft. 2 in. Q,QS in.s$-
fr~m To Fl. in. . s, 1n.
From To Ft. In. in.
. GRAVEL PACK:
Depth Size Material
15.0 3.0 Mortar !l!!!!rtz Sand .,om To Fl.
.om To Ft.
. REMARKS:
STATE WELL CONSTRUCTION
PERMIT NUMBER: 38-0100-WM-0012
County: Granville
' Depth DRILLING LOG
From To Formation DescrlpUon o.o 3.0 Brown Silty Fine Sandx CLAY
3,0 6.0 Brown to Oran~e Clayey Fine
Sand):'. SILT
6,0 9.5 Green to Brown Plastic CLAY
9,5 11.5 Green VeEI Silt:t CLAY
11,5 13,0 Green to Brown SiltI Cls1:e:t
Fine SAND
13,0 14.0 Green to Brown Coarse to Fine
Sand):'. Silt:t CLAY
14 .o 15,0 Green to Brown Clayey Silty
Coarse to Fine SAND
If additional space is needed use back of form.
LOCATION SKETCH
(Show direction and distance from at least two State Roads, or other rnap reference points)
.. -.. ,
' ' • • I I , . , ---........... , ....
I 00 HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15 NCAC 2C. WELL CONSTRUCTION STANDARDS. AND THAT A COPY OF THIS RECORD i'.S BEEN THE ELL OWNER.
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NORTH °CA!l()UNA OEPARTMElfT OF NATUIAI. RE80\llCES AND COMMIHTY OEVB.OPl,EHT
DIVISION OF ElMIIONMENTAI. MANAOEl,ENT -QROIHlWATBI SECTION FOR OFFICE USE ONLY
P.O. BOX 27887 -RALEIOH,N.C. 27811, PHONE [phone] Quad. No. ______ Sertal No. __ _
Lat. Long. ____ Pc_
Minor Basin------------WELL CONSTRUCTION RECORD MW-5 Baeln Code ___________ _ • DRILLING CONTRACTOR ___ s&_ME __ Dr_i_l_l_in_g_c_o_m_p_an_y __
DRILLER REGISTRATION NUMBER --~(}~4~1""2 ____ _
1. WELL LOCATION: (Show skelch of lhe locaJion below)
Oxford Nearest Town: ~-----------------I.., d ... ~ -\-.--, ""D .... I\/ ~
(Road, Communlly, or Subdivision and Loi No.l
2. OWNER __ C_h_a_n_n_e_l_Ma_s_t_e_r_S_a_t_e_l_l_i_t_e_S_y_s_t_e_m_s_,_I_n_c_._
ADDRESS_~P~•_:cO~•....::.Bo~x;.:_1~4~1~6:..__~-~~------
(Street or RoutJt N..o.J Smithfield N.~. 27577
Clly or Town State Zip Code
3. DATE ORILLEfi/3/86-3/4/86 use OF WELL _M_o_n_i_to_r __
4. TOTAL DEPTH 58, 0 1 CUTTINGS COLLECTED Jqlg Yes □No
5. DOES WELL REPLACE EXISTING WELL? 0 Yes KI No
6. STATIC WATER LEVEL: FT. 0 above TOP OF CASING, D below TOP OF CASING IS ~-5-' __ FT. ABOVE LAND SURFACE.
7. YIELD (gpm): _____ METHOD OF TEST ______ _
8. iER ZONES (depth):---------------
9. CHLORINATION: Type ____ _ Amount ______ _
10. CASING:
Wall Thickness
Header Ent. ______ GW-1 Ent. __
STATE WELL CONSTRUCTION PERMIT NUMBER: ___________ _
Granville
County: -----------------,,---
Depth
From o.o To 1 0.5
0.5 . 5 ,5 1
5.5 14. 5'
14,5 17.0 1
17,0 20.0 1
20.0 28.0 1
DRILLING LOG
Gray Si{ty'~'Ji°xrtye~~~~iri (Fill)
Orange-Brown Gravelly Slightly
Sandy Clayey SttT (Fill)
Tan Brown Clayey Slightly Sandy
SILT CFil J}
Dark Gray-Green .Very ·Wet .Slightl~i
Sandy Silty CLAY to Clayey SILT ;
tFill' Orange-Brown Clayey Silty oars<,
I
to Very Coarse SAND (Fill) '
Hard Orange-Tan SILT with Dark
Brown Lamination (Saprolite)
I _2..,8..., • ._,,o._____,_s,..a...,,o._1 Very Dense Dark Brown Silty \
Coarse to Very Coarse SAND with
I lenses cf Metamorphosed Graniti•!
If additional sillme ks ~s.t,,r:laiki tllll)k ol form. I Depth Diameter or Weight/Ft. Material .
0,71//ft, PVC Sh LOCATION SKETCH From -J~,-5 __ To 45, l Fl. 2 -0" c fs~ow direction and distance lrom at least two State Roads, From ---TO ___ Ft. __ _
From To Fl.---
11. GROUT:
From 0.0
From 39 5
12. SCREEN:
Depth
To 39,5 Ft.
Material
01 Portland
Method
Tremmie
To 42, 8 Ft. !,;" Bentonite Pellets
Depth Diameter Slot Size Material
or other map reference points)
From45.l To 55. l Ft. 2.0 in.0,010 In.PVC Sch 40
From ____ To, ___ Ft. ___ in. ___ In. __ _
From To Fl. in. ___ ln. __ _
3. GRAVEL PACK:
Depth Size
•
From 4 2 ,8
From ____ To ___ Ft. _____ _
54 0 Sand To • Ft. ____ _
Material
Quar.tz
"'"'"' ....... .. 4. Rl:MARKS: ________________________________________
_
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15 NCAC 2C, WELL CONSTRUCTION STANDAFlDS, ANO THAT A COPY OF THIS RECORD S BEEN eJ:lE~IED O WELL OWNER.
1W-f Revised 11/84
I.
_.,, .. , ..
•
•
•
Report of the
Installation of Ground Water Monitor Well
Channel Master Satellite Systems, Inc.
Oxford, North Carolina
Prepared for
Channel Master Satellite Systems, Inc.
Smithfield, North Carolina
Prepared by
Soil & Material Engineers, Inc.
Geosciences Department
Cary, North Carolina
March 27, 1986
SOIL & MATERIAL ENGINEERS, INC.
•
•
•
SOIL & MATERIAL ENGINEERS INC. ENGINEERING-TESTING-INSPECTION
1903 Harrison Avenue, Box 609, Cary, NC 27511, Phone [phone]
Channel Master Satelllte Systems, Inc. P. 0, Box 1416
Smithfield, North. Carolina 27.577
Attention: Mr, Felix KIiiette
· March 27, 1986
Reference: Installation of One Ground Water Monitor Well Channel Master Satellite System, Inc. Oxford, North Carolina
S&:ME Job No. 0.5.5-8.5-139-A
Gentlemen:
Soll & Material Engineers, Inc. is pleased to report on the Installation of or,e monitor well at Channel Master Satellite System; Inc, in Oxford, North Carolina. This monitor well was placed approximately In the middle of the original lagoon area,
MONITOR WELL
Upon arrival at the site on March 3, 1986, the drill rig and drill equipment .were steamed deaned to prevent introduction of contaminants into the borehole during drllllng. A CME-.5.5 rotary drill rig was used to drill the borehole. Continuous flight hollow-stem augers (9.5'' O.D.) were used to advance through 19 • .5 feet of sludge and fill material (sludge clay, silt, sand) to the virgin substrate, H-caslng (8.5'' O,D.) was set to 19.8 feet to provide a seal between fill/ sludge material and virgin substrate during drilling. The remainder of the borehole was advanced through weathered rock to .58.0 feet using the washbore method with a roller cone drill bit, Soil samples were taken at 2 • .5 feet intervals in the top 10 feet of virgin substrate and at .5,0 feet intervals thereafter by means of a split barrel sampler in accordance with ASTM D-1.586. These samples were placed in .50 ml VOA bottles, kept on ice, and transported to IEA in Cary, North Carolina for analysis, A field geologist was present to observe the drilling, to sample, and to log the hole, A boring log is presented in the Appendix, The location of the well ls shown on Figure I •
RALEIGH, GREENSBORO, ASHEVILLE, WILMINGTON, FAYETTEVILLE, CHARLOTTE. NC STARTANBURG, COLUMBIA, CHARLESTON, MY.ATLE BEACH, GREENVILLE, SC ATLANTA, ALBANY, ST. MARYS, GA-TRI-CITIES, TN-CINCINNATI, OH-DEERFIELD BEACH. OAIAN[l() TAMPA "'
' t
I
I
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C~el Master Satellite Systems
March Zl, 1986
Page 2
As the drillrod was pulled out of the borehole after completing the drilling
operation, the roller cone drill bit became disconnected and fell to the bottom of the hole,
Efforts to retrieve the bit failed. The roller bit was sealed at the bottom of the hole, A
one foot layer of 0,25 inch bentonite pellet topped by 1.1 feet of concrete size sand was
used to seal the drill bit from the monitor well.
After completion of the borehole, a ground water monitor well was installed as
shown in the Schematic Diagram in the Appendix. The monitor well materials were steam
cleaned before placement in the bo~ehole. In general a 2-inch diameter PVC casing with a
IO-foot long PVC screen was placed in the borehole, The annular space was backfilled
with a concrete· size sand to 3.7 feet above the well screen as determined by a S&ME
geologist. In order to provide a seal against infiltration of surface water along the sides
of the borehole, 3.3 feet of 0.25 inch bentonite pellets were applied on top of the sand
pack. The remaining length of the borehole was grouted in two stages with a neat cement
grout so as to insure an adequate seal between fill material and virgin substrate, The first
grout stage filled the hole up to 17.0 feet and was allowed to set for approximately 16
hours. Then the remainder of the hole was grouted to the ground surface. A protective
steel casing with a lockable cap was grouted in around the top of the monitor well. The
work was completed on March 6, 1986.
SUBSURFACE CONDITIONS
Soil conditions encountered at the boring are shown in the Appendix. In general,
the upper 17.0 feet consisted of orange to brown to dark gray sandy clayey silt followed
by 3 feet of orange-brown sand, This upper 20 feet was considered fill material. A hard
orange-brown silt was encountered from 20-28 feet grading into a very dense dark brown
sand with lenses of metamorphosed granitic rock. The boring terminated in a dark brown
sand.
A copy of the North Carolina Division of Environmental Management Completion
Well Record is included in the Appendix. This log has been sent directly to the State as
required by law •
SOIL & MATERIAL ENGINEERS. INC.
•
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C:::l\aJmel Master Satellite Systems
March 27, 19&6
Page 3
We appreciate the opportunity to have been of service to you, Please contact us"lf
any questions arise regarding this report.
PS/BDT/sws
Sincerely yours,
SOIL &: MATERIAL ENGINEERS, INC.
Perry Sugg
Staff Geologist
Bryson D. Trexler, Jr., Ph.D., P,G,
Senior H ydrogeologist
SOIL l MATERIAL ENGINEERS. INC.
. DEPTH
· FT.
o.o
DESCRIPTION
0.5
14. 5
17.0
20.0
28.0
Orange-Brown Gravelly Slightly Sandy
Clayey SILT (Fill)
Tan-Brown Plastic Clayey Slightly
Sandy SILT (Fill) (ML)
uarK 1.ray-ureen very wet --sllgnt1y ~ana
_.. •, _.,. .... -4 ,r,-• fll /'1:-.J. 1 ,., tMl..t,
Orange-Brown Clayey.Silty Coarse to Verv Coft-ftft C,AIJT\-(Fill) -,~M)
Hard Orange-Tan SILT with Dark Brown
Lamination (Saprolite)
Very Dense Da~k Brown Silty Coarse to
Very Coarse SAND with Lenses of
1-etamorphosed Granitic Rock (Saprolite
•
58.0
Boring Terminated at 58.0 feet
in SAND with Lenses of Metamorphosed
Granitic Rock (Saprolite)
BORING ANO SAMPLING MEETS ASTM 0-1586
.CORE DRILLING MEETS ASTM 0-2113
i PEIETRATION IS THE NlM!ER OF ll.O.VS OF 140 LS. HAMMER
.!.. FALLING 30 IN. REQUIRED TO DRIVE 1.4 IN. 1.D. SAMPLER I FT. •
.\,N)ISTIA!BED SAMPLE -==-WATER TAll.E-24HR.
L.,J ------WATER TAll.E-1 HR. J""1 °/0 ROCK CORE RECX,,,ERY
◄ LOSS OF DRJLLNG WATER
ELEV. 8PEl'ETRATION-Bl.ONS PER Ft
0 10 20 30 '40 60 60 100
--
• 3
10
t ,9
78
• j 8
TEST BORING RECORD
MW-5 BORm NO.
DATE DRILLED 3/3/86-3/4/86
JOB NO. 055-85-139A
SOIL a MATERIAL ENGINEERS, INC.
Well Number: ... MW ... -.. s ______ _ . ~ ' ~
Drilling Metho~: Hollow-Stem/Rotary
Drilling Fluids: Super Gel X Date Started: _ _,3_/3._/_8_6 _______ _
Date Finiahed: __ 3~/ .. 6_/_8_6 ______ _ Static Water Level: _____ Date: ___ _
Geologist/Engineer: Perqr 81108
Remarks: Cool/Partlv cloudy
Observed by:
ALL DEPTHS REFERENCED FROM GROUND SURFACE
O,D, of Borehole: 6.25"
Lockable Cap ------------__
1
_ O.D. of Casing: 2.37~"
Protective Casing
Length of Screen: JOO
Screen Opening Siz•e•:wi.o~;~o~l~Ow11--
Pipe Stickup Distance: 1.5
o.o ...... :-• ____ ...,.m.,r,;'.;;"d::. """'---Elevation of •,• . . . . . . Ground Surface: ______ _
...... =· ~ .. .. . .. . ::,· ... . :::: :·.\-. ... . .. . .. . . . .. . . . . . .. .
(If Known)
ti Eg;ctJ 11;0'1 Grout ··: :::: ---1"f.:: .... .. . . ::::· :-~~--~-:. (Type) ·.·.-: :-.::
2" PVC Sch 40 Casing -:•:: ::::
---,J,,iii,.-i. ~ =-~---....... -:::: (Size & Type) .. ~-····· •:•···· ...... ~ ... ·:.-::
:;;·. •:.,· - --Depth to Top of Bentonite.,· _3_9_._5 __
--Depth to Top of Gravel.,·_4_2_-._s __ _ ., ....
~.' ---Depth to Top of Screen· .,. ------•,;.,. -~
45.1
2" PYC Sch 40 Screen ---+.,..•t!
(Size & Type)
SOIL & MATERIAL ENGINEERS, INC.
· .CARY, NORTH CAROLINA
SCHEMATIC OF MONITOR WELL
. _.J)epth to Bottom of Screen: 55.1' ·
::,;:1,,• :-.:
··.,..:..4:'if·~-58 .o' - --Total Depth: _______ _
PROJECT:
CMO/Chsnnel Master
SCALE: Not To Scale
JOB NO.: O55-85-139A
FIGURE NO,:
•
Industrial & Environmental Analysts, Inc.
P.O. 0ox 12542 • Reseorch Triongle Porli. NC 27709 • 919-467-9919
November 1, 1985
Mr. Buddy Mills
Channel Master
P.O. Box 1416
Smithfield, NC 27577
Reference: IEA Report No. 350-1
Dear Mr. Mills:
-r -
r
Transmitted herewith are the results of analyses on four samples submitted to
our laboratory on October 23, 1985.
Please see the attached sheet for your results .
Very truly yours,
INDUSTRIAL & ENVIRONMENTAL ANALYSTS, INC.
Senior Chemist
JBA/sbm
Enclosure
Offices and loboro1one1 loco1ed in: Essex Junction. Vermont
Reseorch Triangle Park. North Carolina
November 1, 1985
IEA REPORT NO. 350-1
Page 2
• Upstream MW2 MW3 MW4
Total Organic
Halide Rep.I µg/L 20 53 71 360
Total Organic
Halide Rep. 2 µg/L 16 54 71 360
Total Organic
Halide Rep.3 µg/L 16 50 71 360
Total Organic
Halide Rep.4 µg/L 17 51 72 360
Total Organic
Carbon Rep.I mg/L < 1.0 3.3 12 21
Total Organic
Carbon Rep. 2 mg/L < 1.0 3.3 10 21
Total Organic
Carbon Rep.3 mg/L < 1.0 3.3 10 21
To.tal Organic
Carbon Rep.4 mg/L < 1.0 3.3 10 21 • pH Rep. l 6.20 6.55 6.45 6.60
pH Rep,2 6.20 6.70 6.50 6.70
pH Rep.3 6.20 6.65 6.50 6.70
pH Rep.4 6.30 6. 70 . 6.50 6.70
Specific Conductance
Rep. 1 µS/cm 135 1970 1510 1710
Specific Conductance
Rep.2 µS/cm 133 1970 1500 1700
Specific Conductance
Rep. 3 µS/cm 133 2000 1500 1700
/---:t Specific Conductance J Rep.4 µS/cm 134 1980 1510 1710
mg/L < 0.01 < 0.01 < 0.01 < 0.01 Cadmium •I
j Chromium 4.0 mg/L < 0.03 < 0.03 0.04 < 0.03
Nickel 2.ll mg/L < 0.03 0.05 0. 14 0.05 ·(~ Copper 2.1 mg/L < 0.02 < 0.02 0.02 0.02
November 1, 1985
•
IEA REPOR'l\i NO. 350-1
Page 3 JY' j I , \. J Upstream MW2 MW3 MW4
• Arsenic 5 mg/L < 0.005 0.018 0.010 0.021
Barium /VO mg/L < 0.2 < 0.2 < 0. 2 < 0.2
• Lead t; mg/L < 0.005 < 0.005 < 0.005 < 0.005
Selenium 1.0 mg/L < 0.005 < 0.005 < 0.005 < 0.005
Silicon mg/L 26 40 29 18
Mercury o,i. mg/L < 0.002 < 0.002 < 0.002 < 0.002
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Industrial & Environmental Analysts, Inc.
P.O. Dox 12542 • P-eseorch Triangle Porl~. NC 27709 • 919-467-9919
November 11, 1985
Mr. Buddy Mills
Channel Master
P.O. Box 1416
Smithfield, NC 27577
Reference: IEA Report No. 350-2
Dear Mr. Mills:
-
Transmitted herewith are the results of analyses on four samples submitted to
our laboratory on October 29, 1985.
Please see the attached sheets for your results •
Very truly yours, I=1:z:~:AL ::LYSTS,
/2ose';,h B: Adamovic
Senior Chemist
JBA/sbm
Enclosure
INC.
Offices and loborotories located in: Essex Junction, Vermont
i
Research Triangle Pork, North Carolina
November 11, 1985
.l !EA REPORT NO . 350-2
• Total Organic
Upstream MW2 ... MW3 MW4
Halide Rep. l µg/L < 10 41 160 350
Tota_l Organic
Halide Rep.2 µg/L < 10 41 160 350
Total Organic
Halide Rep.3 µg/L < 10 41 160 350
Total Organic
Halide Rep.4 µg/L 12 41 160 j50
Total Organic
Carbon Rep.1 mg/L < 1.0 3.3 25 14
Total Organic
Carbon Rep. 2 mg/L < 1.0 3.3 25 14
Total Organic
Carbon Rep.3 ,, mg/L < 1.0 3.3 25 14
Total Organic
Carbon Rep.4 mg/L < 1.0 3.3 25 14 • pH -Rep. l 6.30 6.70 6.70 6.50
pH -Rep.2 6.30 6.70 6.75 6.55
pH -Rep.3 6.30 6.70 6.75 6.50
pH -Rep.4 6.30 6.70 6.70 6.50
Specific Conductance
Rep. l µS/cm 134 2030 1630 1560
I f Specific Conductance 1· . Rep.2 µS/cm 134 2040 1650 1570 i I-t· Specific Conductance r.
). Rep.3 µS/cm 133 2030 1660 1570 r: I t;
•· Specific_ Conductance i:.
i Rep.4 µS/cm 134 2000 1650 1560 .,
/ Cadmium mg/L < 0.01 < 0.01 < 0.01 < 0.01
Chromium mg/L < 0.03 < 0.03 0.08 < 0.03
Nickel mg/L < 0.03 0.07 0.28 0.04 • Copper mg/L < 0.02 < 0.02 0.05 0.05
November 11, 1985
IEA REPORT NO. 350-2
.\
Page 2
• Upstream MW2 MW3 MW4
Arsenic mg/L < 0.005 < 0.005 < 00 0.021
Barium mg/L < 0.2 < 0.2 < 0.2 < 0.2
Lead mg/L < 0.005 < 0.005 < 0.005 < 0.005
Selenium mg/L < 0.005 < 0.005 < 0.005 < 0.005
Silicon mg/L 26 39 29 18
Mercury mg/L < 0.002 < 0.002 < 0.002 < 0.002
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rn Industrial & Environmental Analysts, Inc.
P.O. Oox 12542
November 15, 1985
Mr. Buddy Mills
Channel Master
P.O. Box 1416
Smithfield, NC 27577
• Research Triangle Parl~.
~ fo
Reference: IEA Report No. 350-3
Dear Mr. Mills:
NC 27709 • 919-467-9919
Transmitted herewith are the results of analyses on four samples submitted to
our laboratory on November 6, 1985.
Please see the attached sheets for your results .
Very truly yours,
INDUSTRIAL & ENVIRONMENTAL ANALYSTS, INC.
~-€a~.::?l:;.ovic~~-C...--
/i~nior Chemist
JBA/sbm
Enclosures
Offices and laboratories located ,n, Essex Junction. Vermont
Research T riongle Park. North Carolina
-,
November 15, 1985
!EA REPORT NO . 350-3
• Upstream MW2 MW3 MW4
Total Organic
Halide Rep.l µg/L 11 57 130 350
Total Organic .6
Halide Rep.2 . ~-µg/L 10 56 130 340
Total Organic i"
Halide Rep.3 µg/L 11 57 130 340
Total Organic
Halide Rep.4 µg/L 11 56 130 340
Total Organic
Carbon Rep.l ~~ mg/L < 1.0 6.5 13 22
Total Organic ~t Carbon Rep.2 mg/L < 1.0 6.5 13 22
Total Organic
Carbon Rep.3 mg/L < 1.0 6.5 13 22
Total Organic
Carbon Rep.4 mg/L < 1.0 6.5 13 22 • pH -Rep.l 5.80 6.60 6.60 6.50
pH -Rep.2 5.90 6.65 6.60 6.55
pH -Rep.3 5.85 6.60 6.60 6.60
pH -Rep.4 5.90 6.60 6.60 6.60
Specific Conductance
Rep.l µS/cm 137 1990 1650 1560
Specific Conductance
Rep.2 µS/cm 136 2020 1680 1540
Specific Conductance
Rep.3 µS/cm 135 2020 1650 1580
Specific Conductance
Rep.4 µS/cm 136 1970 1680 1550
Cadmium ' ·, mg/L < 0.01 < 0.01 < 0.01 < 0.01 , ' '
Chromium .. mg/L < 0.03 < 0.03 < 0.03 < 0.03
Nicke 1 mg/L < 0.03 0.04 0.19 < 0.03 • Copper mg/L < 0.02 < 0.02 < 0.02 0.02
f' . ' November is, 1985
IEA REPORT NO. 350-2
• Page 2
• Upstream MW2 MW3 MW4
Arsenic mg/L < 0.005 < 0.005 < 0.005 < 0.005
Barium ' -·1 ., mg/L < 0.2 < 0.2 < o. 2 < 0.2
Lead ,. .''1 mg/L 0.006 < 0.005 < 0.005 < 0.005 ... : . ;,
Selenium /' () mg/L < 0.005 < 0.005 < 0.005 < 0.005
Silicon mg/L 24 37 28 9.8
·, mg/L < 0.002 < Mercury ,_ . < 0.002 0.002 < 0.002
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Industrial & Environmental Analysts, Inc.
P.O. Clox 12542 • Reseorch Triongle Porl1. NC 27709 • 919-467-9919
November 22, 1985
Mr. Buddy Mills
Channel Master
P.O. Box 1416
Smithfield, NC 27577
Reference: !EA Report No. 350-5
Dear Mr. Mil ls:
$
Transmitted herewith are the results of analyses on four samples submitted to
our laboratory on November 13, 1985.
Please see the attached sheets for your results •
Very truly yours,
INDUSTRIAL & ENVIRONMENTAL ANALYSTS, INC.
~i~ovic
/';::~:~ ~~emist
JBA/sbm
Enclosures
. Offices and loboro1ories located in: Essex Junction, Vermont
Research T riongle Pork. North Carolina
November 2.Z, 1985
IEA REPORT NO. 350-5
U:estream MW2 MW3 MW4 ,. Total Organic
Halide Rep.l µg/L . 16 160 210 340
Total Organic
Halide Rep.2 µg/L 16 150 210 340
Total Organic
Halide Rep.3 µg/L 15 150 210 340
Total Organic
Halide Rep.4 µg/L 15 150 210 340
Total Organic
Carbon Rep.I mg/L < 1.0 6.5 13 22
Total Organic
Carbon Rep.2 mg/L < 1.0 6.5 13 22
Total Organic
Carbon Rep.3 mg/L < 1.0 6.5 13 22
Total Organic
Carbon Rep.4 mg/L < 1.0 6.5 13 22
• pH -Rep. l 6.07 6.53 6.40 6.64
pH. Rep. 2 6.06 6.63 6.47 6.66
pH -Rep.3 6.08 6.65 6.51 6.74
pH. Rep.4 6.10 6.70 6.40 6.75
Specific Conductance
Rep.I µS/cm 139 2000 1600 1700
Specific Conductance
Rep.2 µS/cm 139 1990 1610 1700
Specific Conductance
Rep.3 µS/cm 138 2020 1590 1690
Specific Conductance
Rep.4 µS/cm 139 2010 1610 1710
. -··. Cadmium mg/L < 0.01· < 0.01 < 0.01 < 0.01
Chromium mg/L < 0.03 < 0.03 0.04 < 0.03
Nickel mg/L < 0.03 0.04 0.15 < 0.03 • Copper mg/L < 0.02 < 0.02 ( 0.02 0.02
November 22, 1985
IEA REPORT NO. 350-5
Page 2 ,. Upstream MW2 MW3 MW4
Arsenic mg/L < 0.005 < 0.005 < 0.005 < 0.005
Barium mg/L < 0.2 < 0.2 < 0.2 < 0.2
Lead mg/L < 0.005 < 0.005 < 0.005 < 0.005
Selenium mg/L < 0.005 < 0.005 < 0.005 < 0.005
Silicon . mg/L 24 37 30 16
Mercury mg/L < 0.002 < 0.002 < 0.002 < 0.002
•
•
•
•
• Industrial & Environmental Analysts, Inc.
P.O. Oox 12542 • Research Triangle Pcirk. NC 27709 • 919-467-9919
November 22, 1985
Mr. Buddy Mills
Channel Master
P.O. Box 1416
Smithfield, NC 27577
Reference: IEA Report No. 350-4
Dear Mr. Mills:
Transmitted herewith are the results of analyses on four samples submitted to
our laboratory on November 6, 1985.
Please see the attached sheets for your results •
Very truly yours,
JBA/sbm
Enclosures
.
,-c/4,~i/ly ;f-PA{t(ses__ -z;;
. A"tJi //Ill 1;/~ v,-e11d1iJJ
Offices and laboratories located in: Essex Junction. Vermont
l\eseorch Triangle Pork. North Carolina
VOLATILE FRACTION
CLIENT SAMPLE NO._~U~p~g=r=ad=-1=-· e=n=t-=Sam=p'-'l""e~----
IEA SAMPLE NO. 350-4-3 ------""'-=---'--=---------
NUMBER COMPOUND DETECTION CONCENTRATION
LIMIT (µg/L) (µg/L)
1 ACROLEIN 100 BDL* 2 ACRYLONITRILE 100 BDL 3 BENZENE 10 BDL 4 BROMODICHLOROMETHANE 10 BDL 5 BROMOFORM 10 BDL 6 BROMOMETHANE 10 BDL 7 CARBON TETRACHLORIDE 10 BDL 8 CHLOROBENZENE 10 BDL 9 CHLOROETHANE 10 BDL • 10 2-CHLOROETHYLVINYL ETHER 10 BDL 11 CHLOROFORM 10 BDL 12 CHLOROME'l:!IANE 10 BDL 13 DIBROMOCHLOROMETHANE 10 BDL 14 1,2-DICHLOROBENZENE 10 BDL 15 1,3-DICHLOROBENZENE 10 BDL 16 1,4-DICHLOROBENZENE 10 BDL 17 1,1-DICHLOROETHANE 10 BDL 18 1,2-DICHLOROETHANE 10 BDL 19 1,1-DICHLOROETHENE 10 BDL 20 trans-1,2-DICHLOROETHENE 10 BDL 21 1,2-DICHLOROPROPANE 10 BDL 22 cis-1,3-DICHLOROPROPENE 10 BDL 23 trans-1,3-DICHLOROPROPENE 10 BDL 24 ETHYL BENZENE 10 BDL 25 METHYLENE CHLORIDE 10 BDL 26 1,1,2,2-TETRACHLOROETHANE 10 BDL 27 TETRACHLOROETHENE 10 BDL 28 TOLUENE 10 BDL 29 1,1,1-TRitiltOROETHANE 10 BDL 30 1,1,2-TRICHLOROETHANE 10 BDL 31 TRICHLOROETHENE 10 BDL 32 TRICHLOROFLUOROMETHANE 10 BDL 33 VINYL CHLORIDE 10 BDL • *BDL -BELOW DETECTION LIMIT
•
VOLATILE FRACTION
CLIENT SAMPLE NO. __ _.MW,,,_-..,_2 _________ _
IEA SAMPLE N0 •. ---' ___ 3_50_-_4_-_4 ________ _
NUMBER COMPOUND DETECTION CONCENTRATION
LIMIT (µg/L) (µg/L)
1 ACROLEIN 100 BDL* 2 ACRYLONITRILE 100 BDL 3 BENZENE 10 BDL 4 BROMODICHLOROMETHANE 10 BDL 5 BROMOFORM · 10 BDL 6 BROMOMETHANE 10 BDL 7 CARBON TETRACHLORIDE 10 BDL 8 CHLOROBENZENE 10 BDL 9 CHLOROETHANE 10 BDL 10 2-CHLOROETHYLVINYL ETHER 10 BDL • 11 CHLOROFORM 10 BDL 12 CHLOROMETHANE 10 BDL 13 . DIBROHOCHLiJROMETHANE 10 BDL 14 1,2-DICHLOROBENZENE 10 BDL 15 1,3-DICHLOROBENZENE 10 BDL 16 1,4-DICHLOROBENZENE 10 BDL 17 1,1-DICHLOROETHANE 10 BDL 18 1,2-DICHLOROETHANE 10 BDL 19 1,1-DICHLOROETHENE 10 BDL 20 trans-1,2-DICHLOROETHENE 10 BDL 21 1,2-DICHLOROPROPANE 10 BDL 22 cis-1,3-DICHLOROPROPENE 10 BDL 23 trans-1,3-DICHLOROPROPENE 10 BDL 24 ETHYL BENZENE 10 BDL 25 METHYLENE CHLORIDE 10 BDL 26 1,1,2,2-TETRACHLOROETHANE 10 BDL 27 TETRACHLOROETHENE 10 BDL 28 TOLUENE 10 BDL 29 1,1,l-TRIC~L,9.~Q~THANE 10 BDL 30 1,1,2-TRICHLOROETHANE 10 BDL 31 TRICHLOROETHENE 10 BDL 32 TRICHLOROFLUOROMETHANE 10 BDL 33 VINYL CHLORIDE 10 BDL
*BDL -BELOW DETECTION LIMIT •
• VOLATILE FRACTION
CLIENT SAMPLE NO. MW-3 ---~----------
I EA SAMPLE NO. 350-4-1 ---------------
NUMBER COMPOUND DETECTION CONCENTRATION
LIMIT (µg/L) (µg/L)
1 ACROLEIN 100 BDL*
2 ACRYLONITRILE 100 BDL 3 BENZENE 10 BDL
4 BROMODICHLOROMETHANE 10 BDL
5 BROMOFORM 10 BDL
6 BROMOMETHANE 10 BDL 7 CARBON TETRACHLORIDE 10 BDL
8 CHLOROBENZENE 10 BDL 9 CHLOROETHANE 10 BDL 10 2-CHLOROETHYLVINYL ETHER 10 BDL 11 CHLOROFORM 10 BDL • 12 CHLOROMETHANE 10 BDL
13 DIBROMOCHLOROMETHANE 10 BDL 14 1,2-DICHtOROBENZENE 10 BDL 15 1,3-DICHLOROBENZENE 10 BDL 16 1,4-DICHLOROBENZENE 10 BDL
17 1,1-DICHLOROETHANE 10 BDL 18 1,2-DICHLOROETHANE 10 BDL 19 1,1-DICHLOROETHENE 10 BDL 20 trans-1,2-DICHLOROETHENE 10 BDL 21 1,2-DICHLOROPROPANE 10 BDL 22 cis-1,3-DICHLOROPROPENE 10 BDL 23 trans-1,3-DICHLOROPROPENE 10 BDL 24 ETHYL BENZENE 10 BDL 25 METHYLENE CHLORIDE 10 24. 26 1,1,2,2-TETRACHLOROETHANE 10 BDL 27 TETRACHLOROETHENE 10 BDL 28 TOLUENE 10 BDL 29 1,1,1-TRICHLOROETHANE 10 BDL 30 1,1,2-TR~C!!J,pRpETHANE 10 BDL 31 TRICHLOROETHENE 10 BDL 32 TRICHLOROFLUOROMETHANE 10 BDL 33 VINYL CHLORIDE 10 BDL
*BDL -BELOW DETECTION LIMIT •
•
VOLATILE FRACTION
CLIENT SAMPLE NO. MW-4 ----'=---'-----------
I EA SAMPLE NO. 350-4-2 ---~~~~--------
NUMBER COMPOUND DETECTION CONCENTRATION
LIMIT (µg/L) (µg/L)
l ACROLEIN 100 BDL*
2 ACRYLONITRILE 100 BDL
3 BENZENE 10 BDL
4 BROMODICHLOROMETHANE 10 BDL
5 BROMOFORM I 10 BDL
6 BROMOMETHANE 10 BDL
7 CARBON TETRACHLORIDE 10 BDL
8 CHLOROBENZENE 10 BDL
9 CHLOROETHANE 10 BDL
10 2-CHLOROETHYLVINYL ETHER 10 BDL • 11 CHLOROFORM 10 BDL
12 CHLO ROME THANE 10 BDL
1:1 DIBROMOCHLOROMETHANE 10 BDL
14 1,2-DICHLOROBENZENE 10 BDL
15 1,3-DICHLOROBENZENE 10 BDL
16 1,4-DICHLOROBENZENE 10 BDL
17 1,1-DICHLOROETHANE 10 BDL
18 1,2-DICHLOROETHANE 10 BDL
19 1,1-DICHLOROETHENE 10 BDL
20 trans-1,2-DICHLOROETHENE 10 BDL
21 1,2-DICHLOROPROPANE 10 BDL
22 cis-1,3-DICHLOROPROPENE 10 BDL
23 trans-1,3-DICHLOROPROPENE 10 BDL
24 ETHYL BENZENE 10 BDL
25 METHYLENE CHLORIDE 10 BDL
26 1,1,2,2-TETRACHLOROETHANE 10 BDL
27 TETRACHLOROETHENE 10 BDL
28 TOLUENE 10 BDL
29 1,1,1-TRICHLOROETHANE 10 BDL
30 1,1,2-TRrcm:oROETHANE 10 BDL
31 TRICHLOROETHENE 10 BDL
32 TRICHLOROFLUOROMETHANE 10 BDL
33 VINYL CHLORIDE 10 BDL
*BDL -BELOW DETECTION LIMIT •
•
•
• Industrial & Environmental Analysts, Inc .
P.O. [\ox 12542 • Research Triangle Parl~. NC 27709 • 919-467-9919
November 22, 1985
Buddy Mills
Channel Master
P.O. Box 1416
Smithfield, NC 27577
Reference: IEA Report No. 350-6
Dear Mr. Mills:
Transmitted herewith are the results of analyses on four samples submitted to
our laboratory on November 13, 1985.
Please see the attached sheets for your report •
Very truly yours,
INDUSTRIAL & ENVIRONMENTAL ANALYSTS, INC.
}.t!;~:~
Senior Chemist
JBA/sbm
Enclosures . --/1-:1·.1;; L tf 5 e .s 0 I df!p /,' .;:' j'
/;,j /4 f/,1l 1de f?~c/,'µ d
Offices and laboratories located in: Essex Junction, Vermont
Research T riongle Park. North Carolina
VOLATILE FRACTION
CLIENT SAMPLE NO ._--"U'-"p"'g"-'ra,,,d.,is.,ec,,nc,,t...;S,e,ame!!!!.lp'-'l,ee ____ _
IEA SAMPLE NO. ___ .,,_J,,_5,,_0-~6L-_,l~--------
NUMBER COMPOUNU DETECTION CONCENTRATION
LIMIT (µg/L) (µg/L)
1 ACROLEIN 100 BDL* 2 ACRYLONITRILE 100 BDL 3 BENZENE 10 BDL 4 BROMODICHLOROMETHANE 10 BDL 5 BROMOFORM 10 BDL 6 BROMOMETHANE 10 BDL 7 CARBON TETRACHLORIDE 10 BDL 8 CHLOROBENZENE 10 · BDL 9 CHLOROETHANE 10 BDL 10 2-CHLOROETHYLVINYL ETHER 10 BDL • 11 CHLOROFORM 10 BDL 12 CHLOROMETHANE 10 BDL 13 DIBROMOCHLOROMETHANE 10 BDL 14 1,2-DICHLOROBENZENE 10 BDL 15 1,3-DICHLOROBENZENE 10 BDL 16 1,4-DICHLOROBENZENE 10 BDL 17 1,1-DICHLOROETHANE 10 BDL 18 1,2-DICHLOROETHANE 10 BDL 19 1,1-DICHLOROETHENE 10 BDL 20 trans-1,2-DICHLOROETHENE 10 BDL 21 1,2-DICHLOROPROPANE 10 BDL 22 cis-1,3-DICHLOROPROPENE 10 BDL 23 trans-1,3-DICHLOROPROPENE 10 BDL 24 ETHYL BENZENE 10 BDL 25 METHYLENE CHLORIDE 10 BDL 26 1,1,2,2-TETRACHLOROETHANE 10 BDL 27 TETRACHLOROETHENE 10 BDL 28 TOLUENE 10 BDL 29 1,1,1-TRICHLOROETHANE 10· BDL 30 1,1,2-TRIC!ll,()ROETHANE 10 BDL 31 TRICHLOROETHENE 10 BDL 32 TRICHLOROFLUOROMETHANE 10 BDL 33 VINYL CHLORIDE 10 BDL
*BDL -BELOW DETECTION LIMIT •
•
VOLATILE FRACTION
CLIENT SAMPLE NO._--'MW=..-~2~----------
IEA SAMPLE NO •. _· -~3.,,5"'0'---,,_6-...,2._ ________ _
NUMBER COMPOUND DETECTION CONCENTRATION
LIMIT (µg/L) (µg/L)
1 ACROLEIN 100 BDL*
2 ACRYLONITRILE 100 BDL
3 BENZENE 10 BDL
4 BROMODICHLOROMETHANE 10 BDL
5 BROMOFORM 10 BDL
6 BROMOMETHANE 10 BDL
,7 CARBON TETRACHLORIDE 10 BDL
8 CHLOROBENZENE 10 BDL
9 CHLOROETHANE 10 BDL • 10 2-CHLOROETHYLVINYL ETHER 10 BDL
11 CHLOROFORM 10 BDL
12 CHLOROMETHANE 10 BDL
13 DIBROMOCHLOROMETHANE 10 BDL
14 1,2-DICHLOROBENZENE 10 BDL
15 1,3-DICHLOROBENZENE 10 BDL
16 1,4-DICHLOROBENZENE 10 BDL
17 1,1-DICHLOROETHANE 10 BDL
18 1,2-DICHLOROETHANE 10 BDL 19 1,1-DICHLOROETHENE 10 BDL
20 trans-1,2-DICHLOROETHENE 10 BDL
21 1,2-DICHLOROPROPANE 10 BDL
22 cis-1,3-DICHLOROPROPENE 10 BDL
23 trans-1,3-DICHLOROPROPENE 10 BDL
24 ETHYL BENZENE 10 BDL
25 METHYLENE CHLORIDE 10 BDL
26 1,1,2,2-TETRACHLOROETHANE 10 BDL
27 TETRACHLOROETHENE 10 BDL
28 TOLUENE 10 BDL
29 1,1,1-TRLC!IJ;OROETHANE 10 BDL
30 1,1,2-TRICHLOROETHANE 10 BDL
31 TRICHLOROETHENE 10 BDL
32 TRICHLOROFLUOROIIETHANE 10 BDL
33 VINYL CHLORIDE 10 BDL
*BDL -BELOW DETECTION LIMIT · •
• VOLATILE FRACTION
CLIENT SAMPLE NO. MW-3 --------------
1 EA SAMPLE NO. 350-6-3 ---~~~---------
NUMBER COMPOUND DETECTION CONCENTRATION
LIMIT (µg/L) (µg/L)
1 ACROLEIN. 100 BDL* 2 ACRYLONITRILE 100 BDL 3 BENZENE 10 BDL 4 BROMODICHLOROMETHANE 10 BDL
5 BROMOFORM 10 BDL 6 BROMOMETHANE 10 BDL 7 CARBON TETRACHLORIDE 10 BDL
8 CHLOROBENZENE 10 BDL 9 CHLOROETHANE 10 BDL 10 2-CHLOROETHYLVINYL ETHER 10 BDL
11 CHLOROFORM 10 BDL • 12 CHLO ROME THANE 10 BDL 13 DIBROMOCHLOROMETHANE 10 BDL 14 l,2-DICHL1JROBENZENE 10 BDL 15 1,3-DICHLOROBENZENE 10 BDL 16 1,4-DICHLOROBENZENE 10 BDL 17 1,1-DICHLOROETHANE 10 BDL 18 1,2-DICHLOROETHANE 10 BDL 19 1,1-DICHLOROETHENE 10 BDL 20 trans-1,2-DICHLOROETHENE 10 BDL 21 1,2-DICHLOROPROPANE 10 BDL 22 cis-1,3-DICHLOROPROPENE 10 BDL 23 trans-1,3-DICHLOROPROPENE 10 BDL
24 ETHYL BENZENE 10 BDL 25 METHYLENE CHLORIDE 10 BDL 26 1,1,2,2-TETRACHLOROETHANE 10 BDL 27 TETRACHLOROETHENE 10 BDL 28 TOLUENE 10 BDL 29 1,1,1-TRICHLOROETHANE 10 BDL 30 1,1,2-TRICHLOROETHANE 10 BDL 31 TRICHLOROETHENE 10 BDL 32 TRICHLOROFLUOROMETHANE 10 BDL 33 VINYL CHLORIDE 10 BDL
*BDL -BELOW DETECTION LIMIT •
. '
•
VOLATILE FRACTION
CLIENT SAMPLE NO. MW-4 --=~----------
1 EA SAMPLE NO. ___ ~3~5O~-~6~-~4 ________ _
NIJM1!ER COMPOUND DETECTION CONCENTRATION
LIMIT (µg/L) (µg/L)
1 ACROLEIN 100 BDL* 2 ACRYLONITRILE 100 BDL 3 BENZENE 10 BDL 4 BROMODICHLOROMETHANE 10 BDL 5 BROMOFORM 10 BDL 6 BROMOMETHANE 10 BDL 7 CARBON TETRACHLORIDE 10 BDL 8 CHLOROBENZENE 10 BDL • 9 CHLO ROE THANE 10 BDL 10 2-CHLOROETHYLVINYL ETHER 10 BDL • 11 CHLOROFORM 10 BDL 12 CHLOROMETHANE 10 BDL 13 DIBROMOCULOROMETHANE 10 BDL 14 1,2-DICHLOROBENZENE 10 BDL 15 1,3-DICHLOROBENZENE 10 BDL 16 1,4-DICHLOROBENZENE 10 BDL 17 1,1-DICHLOROETHANE 10 BDL 18 1,2-DICHLOROETHANE 10 BDL 19 1,1-DICHLOROETHENE 10 BDL 20 trans-1,2-DICHLOROETHENE 10 BDL 21 1,2-DICHLOROPROPANE 10 BDL 22 cis-1,3-DICHLOROPROPENE 10 BDL 23 trans-1,3-DICHLOROPROPENE 10 BDL 24 ETHYL BENZENE 10 BDL 25 METHYLENE CHLORIDE 10 BDL 26 1,1,2,2-TETRACHLOROETHANE 10 BDL 27 TETRACHLOROETHENE 10 BDL 28 TOLUENE 10 BDL 29 1,1,1-TRICHLOROETHANE 10 BDL 30 1,1,2-TR?Cl!LDROETHANE 10 BDL 31 TRICHLO~OETHENE 10 BDL 32 TRICHLOROFLUOROMETHANE 10 BDL 33 VINYL CHLORIDE 10 BDL
*BDL -BELOW DETECTION LIMIT •
' .
•
•
.;;z,t--1'4~
Industrial & Environmental Analysts, Inc.
P.O. 0ox 12542 • fl-eseorch Triongle Porl,, NC 27709 • 919-467-9919
December 9, 1985
Buddy Mills
Channel Master
P.O. Box 1416
Smithfield, NC 27577
Reference: !EA Report No. 350-7
Dear Mr. Mills:
Transmitted herewith are the results of analyses on four samples submitted to our laboratory on December 6, 1985.
Please see the'attached sheets for your results •
JBA/sbm
/l-f-J ;;L 1 [ f: $ t; I ;[eJi iy
/2,g't, !f-*,cle v.e.1,1dtvj
Offices and laboratories located in: Essex Junction. Vermont 11.eseorch Triangle Pork. North Carolina
BASE/NEUTRAL FRACTION
CLIENT SAMPLE NO. Upgradient
IEA SAMPLE NO . 350-7-1 • NUMBER COMPOUNDS DETECTION LIMIT CONCENTRATII
(µg/1) (µg/1)
l ACENAPHTHENE 25 BDL* 2 ACENAPHTHYLENE 10 BDL 3 ANTHRACENE 10 BDL 4 BENZIDINE 10 BDL 5 BENZO {a) ANTHRACENE 10 BDL 6 BENZO (a) PYRENE 10 BDL 7 BENZO (b) FLUORANTHENE 10 BDL 8 BENZO (ghi) PERYLENE 25 BDL 9 BENZO (k) FLUORANTHENE 10 BDL 10 BIS(2-Cl!LOROETHOXY)METHANE 10 BDL 11 BIS(2-CHLOROETHYL)ETl!ER 10 BDL 12 BIS(2-CHLOROISOPROPYL)ETHER 10 BDL 13 BIS(2-ETHYLHEXYL)PHTHALATE 10 BDL 14 4-BROMOPHENYL PHENYL ETHER 10 BDL 15 BENZYL BUTYL PHTIIALATE 10 BDL 16 2-CHLORONAPHTHALENE 10 BDL 17 4-CHLOROPHENYL PHENYL ETHER 10 BDL 18 CHRYSENE 10 BDL 19 DIBENZO (a,h) ANTHRACENE 25 BDL 20 1,2 DICHLOROBENZENE 10 BDL 21 1,3 DICHLOROBENZENE 10 BDL 22 1,4 DICHLOROBENZENE 10 BDL • 23 3,3'-DICHLOROBENZIDINE 10 BDL 24 DIETHYL PHTHALATE 10 BDL 25 DIMETHYL PHTHALATE 10 BDL 26 DI-N-BUTYL PHTHALATE 10 BDL 27 2,4-DINITROTOLUENE 10 BDL 28 2,6-DINITROTOLUENE 10 BDL 29 DI-N-OCTYL PHTHALATE 10 BDL 30 FLUORANTHENE 10 BDL 31 FLUORENE 10 BDL 32 HEXACHLOROBENZENE 10. BDL 33 HEXACHLOROBUTADIENE · 10 BDL 34 HEXACHLOROCYCLOPENTADIENE 10 BDL 35 HEXACHLOROETHANE 10 BDL 36 INDENO(l,2,3-cd)PYRENE 25 BDL 37 ISOPHORONE 10 BDL 38 NAPHTHALENE 10 BDL 39 NITROBENZENE 10 BDL 40 N-NITROSODIMETHYLAMINE 10 BDL 41 N-NITROSO-DI-N-PROPYLAMINE 10 BDL 42 N-NITROSODIPHENYLAMINE 10 BDL 43 PHENANTHRENE 10 BDL 44 PYRENE 10 BDL 45 1,2,4-TRICHLOROBENZENE 10 BDL
*BDL -BELOW DETECTION LIMIT •
BASE/NEUTRAL FRACTION
CLIENT SAMPLE NO. MW 2
IEA SAMPLE NO. J5Q-Z-2 • NUMBER COMPOUNDS DETECTION LIMIT CONCENTRATim
(µg/1) (µg/1)
1 ACENAPHTHENE 25 BDL* 2 ACENAPHTHYLENE 10 BDL 3 ANTHRACENE 10 BDL 4 BENZIDINE 10 BDL 5 BENZO (a) ANTHRACENE 10 BDL 6 BENZO (a) PYRENE 10 BDL 7 BENZO (b) FLUORANTHENE 10 BDL 8 BENZO (ghi) PERYLENE 25 BDL 9 BENZO (k) FLUORANTHENE 10 BDL 10 BIS(2-CHLOROETHOXY)METHANE 10 BDL 11 BIS(2-CHLOROETHYL)ETHER 10 BDL 12 BIS(2-CHLOROISOPROPYL)ETHER 10 BDL 13 BIS ( 2-ETHYLHEXYL) PHTHALATE. 10 BDL 14 4-BROMOPHENYL PHENYL ETHER 10 BDL 15 BENZYL BUTYL PHTHALATE 10 BDL 16 2-CHLORONAPHTHALENE 10 BDL 17 4-CHLOROPHENYL PHENYL ETHER 10 BDL 18 CHRYSENE 10 BDL 19 DIBENZO (a,h) ANTHRACENE 25 BDL 20 1,2 DICHLOROBENZENE 10 BDL 21 1,3 DICHLOROBENZENE 10 BDL 22 ·1,4 DICHLOROBENZENE 10 BDL • 23 3,3'-DICHLOROBENZIDINE 10 BDL 24 DIETHYL PHTHALATE 10 BDL 25 DIMETHYL Pl!THALATE 10 BDL 26 DI-N-BUTYL PHTHALATE 10 BDL 27 2,4-DINITROTOLUENE 10 BDL 28 2,6-DINITROTOLUENE 10 BDL 29 DI-N-OCTYL PHTHALATE 10 BDL 30 FLUORANTHENE 10 BDL 31 FLUORENE 10 BDL 32 HEXACHLOROBENZENE 10 BDL 33 HEXACHLOROBUTADIENE 10 BDL 34 HEXACHLOROCYCLOPENTADIENE 10 BDL 35 HEXACHLOROETHANE 10 BDL 36 INDENO(l,2,3-cd)PYRENE 25 BDL 37 ISOPHORONE 10 BDL 38 NAPHTHALENE 10 BDL 39 NITROBENZENE 10 BDL 40 N-NITROSODIMETHYLAMINE 10 BDL 41 N-NITROSO-DI-N-PROPYLAMINE 10 BDL 42 N-NITROSODIPHENYLAMINE 10 . BDL 43 PHENANTHRENE 10 BDL 44 PYRENE 10 BDL 45 1,2,4-TRICHLOROBENZENE 10 BDL
*BDL -BELOW DETECTION LIMIT •
BASE/NEUTRAL FRACTION
CLIENT SAMPLE NO. MW 3
IEA SAMPLE NO. 350-7-3 • NUMBER COMPOUNDS DETECTION LIMIT CONCENTRATION
(µg/1) (µg/1)
l ACENAPHTHENE 25 BDL* 2 ACENAPHTHYLENE 10 BDL 3 ANTHRACENE 10 BOL 4 BENZIDINE 10 BDL 5 BENZO (a) ANTHRACENE 10 BDL 6 BENZO (a) PYRENE 10 BDL 7 BENZO (b} FLUORANTHENE 10 BDL 8 BENZO (ghi) PERYLENE 25 BDL 9 BENZO (k} FLUORANTHENE 10 BDL 10 BIS(2-CHLOROETHOXY)METHANE 10 BDL 11 BIS(2-CHLOROETHYL)ETIIER 10 BDL 12 BIS(2-CHLOROISOPROPYL)ETHER 10 BDL 13 BIS(2-ETHYLHEXYL)PHTHALATE· 10 BDL 14 4-BROMOPHENYL PHENYL ETHER 10 BDL 15 BENZYL BUTYL PIITHALATE 10 BDL 16 2-CHLORONAPHTHALENE 10 BDL 17 4-CHLOROPHENYL PHENYL ETHER 10 BDL 18 CHRYSENE 10 BDL 19 DIBENZO (a,h) ANTIIRACENE 25 BDL 20 1,2 DICHLOROBENZENE 10 BDL 21 1,3 DICHLOROBENZENE 10 BDL • 22 1,4 DICHLOROBENZENE 10 BDL 23 3,3'-DICHLOROBENZIDINE 10 BDL 24 DIETHYL PHTHALATE 10 BDL 25 DIMETHYL PHTHALATE 10 BDL 26 DI-N-BUTYL PIITHALATE 10 BDL 27 2,4-DINITROTOLUENE 10 BDL 28 2,6-DINITROTOLUENE 10 BDL 29 D1-N-OCTYL PHTHALATE 10 BDL 30 FLUORANTHENE 10 BDL 31 FLUORENE 10 BDL 32 HEXACHLOROBENZENE 10 BDL 33 HEXACHLOROBUTADIENE 10 BDL 34 HEXACHLOROCYCLOPENTADIENE 10 BDL 35 HEXACHLOROETHANE 10 BDL 36 INDENO(l,2,3-cd)PYRENE 25 BDL 37 ISOPIIORONE 10 BDL 38 NAPHTHALENE 10 BDL 39 NITROBENZENE 10 BDL 40 N-NhTROSODIMETHYLAMINE 10 BDL 41 N-NITROSO-DI-N-PROPYLAMINE 10 BDL 42 N-NITROSODIPHENYLAMINE 10 ·BDL 43 PHENANTHRENE 10 BDL 44 PYRENE 10 BDL 45 1,2,4-TRICIILOROBENZENE 10 BDL
*BDL -BELOW DETECTION LIMIT •
BASE/NEUTRAL FRACTION
CLIENT SAMPLE NO. MW 4
IEA SAMPLE NO. 350-7-4 ,. NUMBER COMPOUNDS DETECTION LIMIT CONCENTRATION
(µg/1) (µg/1)
1 ACENAPHTHENE 25 BDL* 2 ACENAPHTHYLENE 10 BDL 3 ANTHRACENE 10 BDL 4 BENZIDINE 10 BDL 5 BENZO (a) ANTHRACENE 10 BDL 6 BENZO (a) PYRENE 10 BDL 7 BENZO (b) FLUORANTHENE 10 BDL 8 BENZO (ghi) PERYLENE 25 BDL 9 BENZO (k) FLUORANTHENE 10 BDL 10 BIS(2-CHLOROETHOXY)METHANE 10 BDL 11 BIS(2-CHLOROETHYL)ETHER 10 BDL 12 BIS(2-CHLOROISOPROPYL)ETHER 10 BDL 13 BIS(2-ETHYLHEXYL)PHTHALATE 10 BDL 14 4-BROMOPHENYL PHENYL ETHER 10 BDL 15 BENZYL BUTYL PHTHALATE 10 BDL 16 2-CHLORONAPHTHALENE 10 BDL 17 4-CHLOROPHENYL PHENYL ETHER 10 BDL 18 CHRYSENE 10 BDL 19 DIBENZO (a,h) ANTHRACENE 25 BDL 20 1,2 DICHLOROBENZENE 10 BDL 21 1,3 DICHLOROBENZENE 10 BDL 22 1,4 DICHLOROBENZENE 10 BDL • 23 3,3'-DICHLOROBENZIDINE 10 BDL 24 DIETHYL PHTHALATE 10 BDL 25 DIMETHYL PHTHALATE 10 BDL 26 DI-N-BUTYL PHTHALATE 10 BDL 27 2,4-DINITROTOLUENE 10 BDL 28 2,6-DINITROTOLUENE 10 BDL 29 DI-N-OCTYL PHTHALATE 10 BDL 30 FLUORANTHENE 10 BDL 31 FLUORENE 10 BDL 32 HEXACHLOROBENZENE 10 BDL 33 HEXACHLOROBUTADIENE 10 BDL 34 HEXACHLOROCYCLOPENTADIENE 10 BDL 35 HEXACHLOROETHANE 10 BDL 36 INDENO(l,2,3-cd)PYRENE 25 BDL 37 ISOPHORONE 10 BDL 38 NAPHTHALENE 10 BDL 39 NITROBENZENE 10 BDL 40 N-NITROSODIMETHYLAMINE 10 BDL 41 N-NITROSO-DI-N-PROPYLAMINE 10 BDL 42 N-NITROSODIPHENYLAMINE 10 .. BDL 43 PHENANTHRENE 10 BDL 44 PYRENE 10 BDL 45 1,2,4-TRICHLOROBENZENE 10 BDL
*BDL -BELOW DETECTION LIMIT •
I'
•
•
•
I tJ• 1
.;;::t,.f'..c.~
Industrial & Environmental Analysts, Inc.
P.O. 0ox 12542 • Reseorch Triongle Porl,. NC 27709 • 919-467-9919
December 9, 1985
Buddy Mills
Channel Master
P.O. Box 1416
Smithfield, NC 27577
Reference: IEA Report No.. 350-7
Dear Mr. Mills:
Transmitted herewith are the results of analyses on four samples submitted to our laboratory on December 6, 1985.
Please see the·~ttached sheets for your results .
Very truly yours,
INDUSTRIAL & ENVIRONMENTAL ANALYSTS, INC. ~-e-mo~ F~~~~~~ ~~~mist
JBA/sbm
Offices and laboratories located in: Essex Junction. Vermont
Research Triangle Pork. North Carolina
• PESTICIDE FRACTION
CLIENT SAMPLE NO. Upgradient
IEA SAMPLE NO. 350-7-1
NUMBER COMPOUNDS DETECTION LIMIT CONCENTRATION
(µg/L) (µg/L)
1 ALDRIN 10 BDL*
2 alpha -BHC 10 BDL
3 Beta -BHC 10 BDL
4 Delta -BHC 10 BDL
5 Gamma -BHC 10 BDL
6 CHLORDANE 10 BDL
7 4,4'-DDD 10 BDL
8 4,4°-DDE 10 BDL
9 4,4'-DDT 10 BDL
10 DIELDRIN 10 BDL
11 ENDOSULFAN I 10 BDL
12 ENDOSULFAN II 10 BDL
13 ENDOSULFAN SULFATE 10 BDL
14 ENDRIN 10 BDL • 15 ENDRIN ALDEHYDE 10 BDL
16 HEPTACHLOR 10 BDL
17 HEPTACHLOR EPOXIDE 10 BDL
18 TOXAPHENE 10 BDL
19 PCB 1016 10 BDL
20 PCB 1221 10 BDL
21 PCB 1232 10 BDL
22 PCB 1242 10 BDL
23 PCB 1248 10 BDL
24 PCB 1254 10 BDL
25 PCB 1260 10 BDL
*BDL -BELOW DETECTION LIMIT
•
• PESTICIDE FRACTION
CLIENT SAMPLE NO. Mw 2
IEA SAMPLE NO. 350-7-2
NUMBER COMPOUNDS DETECTION LIMIT CONCENTRATION
(µg/L) (µg/L)
1 ALDRIN 10 BDL*
2 alpha -BHC 10 BDL
3 Beta -BHC 10 BDL
4 Delta -BHC 10 BDL
5 Gamma -BHC 10 BDL
6 CHLORDANE 10 BDL
7 4,4'-DDD 10 BDL
8 4,4'-DDE 10 BDL
9 4,4'-DDT 10 BDL
10 DIELDRIN 10 BDL
11 ENDOSULFAN I 10 BDL
12 ENDOSULFAN II 10 BDL
13 ENDOSULFAN SULFATE 10 BDL
14 ENDRIN 10 BDL • 15 ENDRIN ALDEHYDE 10 BDL
16 HEPTACHLOR 10 BDL
17 HEPTACHLOR EPOXIDE 10 BDL
18 TOXAPHENE 10 BDL
19 PCB 1016 10 BDL
20 PCB 1221 10 BDL
21 PCB 1232 10 BDL
22 PCB 1242 10 BDL
23 PCB 1248 10 BDL
24 PCB 1254 10 BDL
25 PCB 1260 10 BDL
*BDL -BELOW DETECTION LIMIT
•
'. ,.
• PESTICIDE FRACTION
CLIENT SAMPLE NO.
IEA SAMPLE NO. 350-7-3
NUMBER COMPOUNDS DETECTION LIMIT CONCENTRATION
(µg/L) (µg/L)
1 ALDRIN 10 BDL* 2 alpha -BHC 10 BDL 3 Beta -BHC 10 BDL 4 Delta -BHC 10 BDL 5 Gamma -BHC 10 BDL 6 CHLORDANE 10 BDL
7 4,4'-DDD 10 BDL 8 4,4'-DDE 10 BDL 9 4,4'-DDT 10 BDL
10 DIELDRIN 10 BDL 11 ENDOSULFAN I 10 BDL 12 ENDOSULFAN II 10 BDL 13 ENDOSULFAN SULFATE 10 BDL 14 ENDRIN 10 BDL 15 ENDRIN ALDEHYDE 10 BDL • 16 HEPTACHLOR 10 BDL
17 HEPTACHLOR EPOXIDE 10 BDL 18 TOXAPHENE 10 BDL 19 PCB 1016 10 BDL
20 PCB 1221 10 BDL 21 PCB 1232 10 BDL 22 PCB 1242 10 BDL
23 PCB 1248 10 BDL
24 PCB 1254 10 BDL
25 PCB 1260 10 BDL
*BDL -BELOW DETECTION LIMIT
•
,. ' '.
•
•
•
PESTICIDE FRACTION
CLIENT SAMPLE NO. MW 4
IEA SAMPLE NO. 350-7-4
NUMBER COMPOUNDS DETECTION LIMIT
(µg/L)
1 ALDRIN 10 2 alpha -BHC 10 3 Beta -BHC 10 4 Delta -BHC 10 5 Gamma -BHC 10 6 CHLORDANE 10 7 4,4'-DDD 10 8 4,4'-DDE 10 9 .4,4' ~DDT 10 10 DIELDRIN 10 11 ENDOSULFAN I 10 12 ENDOSULFAN II 10 13 ENDOSULFAN SULFATE 10 14 ENDRIN 10 15 ENDRIN .ALDEHYDE 10 16 HEPTACHLOR 10 17 HEPTACHLOR EPOXIDE 10 18 TOXAPHENE 10 19 PCB 1016 10 20 PCB 1221 10 21 PCB 1232 10 22 PCB 1242 10 23 PCB 1248 10 24 PCB 1254 10 25 PCB 1260 10
*BDL -BELOW DETECTION LIMIT
CONCENTRATION
(µg/L)
BDL*
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
•
•
•
rn .;.Z<'4-i',
Industrial & Environmental Analysts, Inc.
P.O. 0ox 12542 • Reseorch Triangle Porl1. NC 27709 • 919-467-9919
December 9, 1985
Buddy Mills
Channel Master
P.O. Box 1416
Smithfield, NC 27577
Reference: IEA Report No, 350-7
Dear Mr. Mills:
Transmitted herewith are the results of analyses on four samples submitted to our laboratory on December 6, 1985.
Please see the.·?ttached sheets for your results •
Very truly yours,
INDUSTRIAL & ENVI~ONMENTAL ANALYSTS, INC. ~-lo~ ~:=~~: ~~~mist
JBA/sbm
Offices and laboratories located in: Essex Junction. Vermont
Research Triangle Pork. North Carolina
• ACID FRACTION
CLIENT SAMPLE NO •. ___ U:._pg:..r_a_d_i_e_n_t _______ _
IEA SAMPLE NO. ___ J_s_o_-_1_-_1 _______ _
NUMBER COMPOUNDS DETECTION LIMIT CONCENTRATION
(µg/1) (µg/1)
1 4-CHLOR0-3-METHYLPHENOL 25 BDL*
2 2-CHLOROPHENOL 25 BDL
3 2,4-DICHLOROPHENOL 25 BDL
4 2,4-DIMETHYLPHENOL 25 BDL
5 2,4-DINITROPHENOL 250 BDL
6 2-METHYL-4,6-DINITROPHENOL 250 BDL
7 2-NITROPHENOL 25 BDL
8 4-NITROPHENOL 25 BDL • 9 PENTACHLOROPHENOL 25 BDL
10 PHENOL 25 BDL
11 2,4,6-TRICHLOROPHENOL 25 BDL
*BDL -BELOW DETECTION LIMIT
•
•
ACID FRACTION
CLIENT SAMPLE NO. __ ....n,.___.._ _________ _
IEA SAMPLE NO. 350-7-2 --------------
NUMBER COMPOUNDS DETECTION LIMIT CONCENTRATION
(µg/1) (µg/1)
1 4-CHLOR0-3-METHYLPHENOL 25 BDL* 2 2-CHLOROPHENOL 25 BDL 3 2,4-DICHLOROPHENOL 25 BDL
4 2,4-DIMETHYLPHENOL 25 BDL 5 2,4-DINITROPHENOL 250 BDL 6 2-METHYL-4,6-DINITROPHENOL 250 BDL • 7 2-NITROPHENOL 25 BDL
8 4-NITROPHENOL 25 BDL
9 PENTACHLOROPHENOL 25 BDL 10 PHENOL 25 BDL 11 2,4,6-TRICHLOROPHENOL 25 BDL
*BDL -BELOW DETECTION LIMIT
•
• ACID FRACTION
CLIENT SAMPLE NO. MW 3 --------------
IEA SAMPLE NO. -JS0-7-3 ------'---------
NUMBER COMPOUNDS DETECTION LIMIT CONCENTRATION
(µg/1) (µg/1)
1 4-CHLOR0-3-METHYLPHENOL 25 BDL* 2 2-CHLOROPHENOL 25 BDL 3 2,4-DICHLOROPH~NOL 25 BDL 4 2,4-DIMETHYLPHENOL 25 BDL 5 2,4-DINITROPHENOL 250 BDL 6 2-METHYL-4,6-DINITROPHENOL 250 BDL 7 2-NITROPHENOL 25 BDL
8 4-NITROPHENOL 25 BDL • 9 PENTACHLOROPHENOL 25 BDL 10 PHENOL 25 BDL 11 2,4,6-TRICHLOROPIIENOL 25 BDL
*BDL -BELOW DETECTION LIMIT
•
•
ACID FRACTION
CLIENT SAMPLE NO. MW 4 ---------------
IEA SAMPLE NO. 350-7-4 --------------
NUMBER COMPOUNDS DETECTION LIMIT CONCENTRATION
(µg/1) (µg/1)
1 4-CHLOR0-3-METHYLPHENOL 25 BDL* 2 2-CHLOROPHENOL 25 BDL 3 2,4-DICHLOROPHENOL 25 BDL 4 2,4-DIMETHYLPHENOL 25 BDL 5 2,4-DINITROPHENOL 250 BDL 6 2-METHYL-4,6-DINITROPHENOL 250 BDL
7 2-NITROPHENOL 25 BDL • 8 4-NITROPHENOL 25 BDL
9 PENTACHLOROPHENOL 25 BDL 10 PHENOL 25 BDL 11 2,4,6-TRICHLOROPHENOL 25 BDL
*BDL -BELOW DETECTION LIMIT
•
•
•
•
rn Industrial & Environmental Analysts, Inc. P.O. 0ox 12542 • Research Triangle Parl~. NC 27709 • 919-467-9919
December 18, 1985
Buddy Mills
Channel Master
P.O. Box 1416
Smithfield, NC 27577
Reference: !EA Report No. 350-3A
Dear Mr. Mills:
Transmitted_ herewith are the results of analyses on four samples submitted to our laboratory on December 18, 1985. The values reported below substantiate the potential interference we discussed concerning the total organic halide (TOX) result on your monitoring wells.
Inorganic halide at levels 2000 to 20,000 higher than the TOX value may yield false positives as listed in both EPA Method 450.l and SW846/9020.
Up-Gradient
Chloride mg/L 8.5
MW2
44
MW3
38
MW4
84
If I may be of any further assistance in this matter, please contact me at the above number.
Very truly yours,
INDUSTRIAL & ENVIRONMENTAL ANALYSTS, INC.
(/M~fr3-~
Me~h B. Adamo·,ic ~ Senior Chemist
JBA/sbm
Offices and laboratories located in: Essex Junction. Vermont
P.eseorch Triangle Pork, North Carolina
••
•
Industrial & Environmental Analysts, Inc.
P.O. Oox 12542 • Research Triangle Parl~. NC 27709 • 919-467-9919
March 20, 1986
Felix Killette
Channel Master Co.
P.O. Box 1416
Smithfield, NC 23994
Reference: IEA Report No, 115-46
Dear Mr. Killette:
Transmitted herewith are the results of analyses on eight samples submitted to our laboratory on March 6, 1986.
The extraction procedure toxicity was performed according to SW846 Method 1310.
Please see the attached reports for your results.
Very truly yours,
INDUSTRIAL & ENVIRONMENTAL ANALYSTS,
14//ij_~~
/Jo;eph B. Adamovic
Senior Chemist
JBA/sbm
Enclosures
INC,
,,
Offices and laboratories located in: Essex Junction, Vermont
Reseorch Triongle Park. North Carolino
• VOLATILE FRACTION ~ w111e-r
CLIENT SAMPLE NO. MW-5
IEA SAMPLE NO. 115-46-9
NUMBER COMPOUND DETECTION CONCENTRATION
LIMIT (µg/L) (µg/L)
1 ACROLEIN 300 BDL* 2 ACRYLONITRILE 300 BDL 3 BENZENE 30 BDL 4 BROMODICHLOROMETHANE 30 BDL 5 BROMOFORM 30 BDL 6 BROMOMETHANE 30 BDL 7 CARBON TETRACHLORIDE 30 BDL 8 CHLOROBENZENE 30 BDL 9 CHLO ROE THANE 30 BDL 10 2-CHLOROETHYVINYL ETHER 30 BDL 11 CHLOROFORM 30 BDL 12 CHLO ROME THANE 30 BDL 13 DIBROMOCHLOROMETHANE 30 BDL • 14 1,2-DICHLOROBENZENE 30 BDL 15 1,3-DICHLOROBENZENE 30 BDL 16 1,4-DICHLOROBENZENE 30 BDL 17 1,1-DICHLOROETHANE 30 BDL 18 1,2-DICHLOROETHANE 30 BDL 19 1,1-DICHLOROETHENE 30 BDL 20 trans-1,2-DICHLOROETHENE 30 BDL 21 1,2-DICHLOROPROPANE 30 BDL 22 cis-1,3-DICHLOROPROPENE 30 BDL 23 trans-1,3-DICHLOROPROPENE 30 BDL 24 ETHYL BENZENE 30 BDL 25 METHYLENE CHLORIDE 30 BDL 26 1,1,2,2-TETRACHLOROETHANE. 30 BDL 27 TETRACHLQBOEIHENE ., 30 I 950. 28 TOLUENE 30: 30. 29 1,1,1-TRICHLOROETHANE 30 BDL 30 1,1,2-TRICHLOROETHANE 30 BDL 31 ...IB!CHIOROEIHENE 30 7000. 32 TRICHLOROFLUOROMETHA~ 30 BDL 33 VINYL CHLORIDE 30 BDL
*BDL -Below Detection Limit ,.
Sample diluted by 5 due to a higtl concentration of trichloroethane . • ·,
• •
March 20, 1986
IEA Report No. 115-46
MW-5 MW-5 MW-5 MW-5 MW-5 MW-5 MW-5 MW-5
19.5-21.0 23.5-24.8 26.0-27.5 28.5-30.0 33.5-34.4 38.5-38.9 43.5-43.8 53.5-55.0
EP-TOX Arsenic mg/L < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 NO < 0.005
EP-Tox. Barium mg/L < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 ------< 0.2 ...
EP-TOX Cadmium,. mg/L < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 ------< 0.01
EP-TOX Chromium Jllg/L .. -< 0.03 < 0.03 < 0.03 < 0.03 < 0.03 < 0.03 ------< 0.03
EP-TOX Lead mg/L < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 SAMPLE < 0.005
.:
EP-TOX Mercury mg/L < 0.0.005 < 0.0005 < 0.0005 < 0.0005 < 0.0005 < 0.0005 ------< 0.0005
EP-TOX Selen.ium mg/L < 0.005 < 0. oos.. < 0.005 < 0.005 . < 0.005 < 0.005 ------< 0.005
EP-TOX Silver mg/L < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 SUBMITTED < 0.05
'·
•• SAMPLE I. D. ___ MW"'---"'-5---'l::..:9_; • ..c.5_-,;:_2,;:_l'--. O'-------
DATE ANALYZED_~3~/1=8~/~8~6 _____ BY ·Randall
VOLUME ANALYZED 2.0
COMPOUND CONCENTRATION
µg/kg
Chloromethane < 10
Bromomethane < 10
Vinyl Chloride < 10
Dichlorodifluormethane < 10
Chloroethane < 10
Methylene Chloride < 10
Trichlorofluormethane < 10
1,1-Dichloroethylene < 10
1,1-Dichloroethane < 10
+-1,2-Dichloroethylene < 10 • Chloroform < 10
1,2-Dichloroethane < 10
1, 1, 1-Trich lo roe thane• < 10
Carbon Tetrachloride < 10
Bromodichloromethane < 10
1,2-Dichloropropane < 10
+-1,3-Dichloropropene < 10
Trichloroethylene < 10
c-1,3-Dichloropropene ., < 10
1,1,2-Trichloroethane < 10 ., Chlorodibromomethane •; < 10
2-Chloroethyl vinyl ether < 10
Bromoform /~-< 10
1,1,2,2-Tetrachloroethylene < 10
l,l,2,2-Tetrachlor.9ethane < 10
Chlorobenzene < 10 • 1,3-Dichlorobenzene < 10
" < 10 1,2-Dichlorobertzene
1, 4-Dichlor_obenzene < 10
•
•
SAMPLE I.D._......cMW=--=5---'2=3~·c.=5_-=2~4"-.8'--------
DATE ANALYZED 3-18-86 BY Randall ----------
VOLUME ANALYZED _____ 2=.0"--'"-------
COMPOUND CONCENTRATION
µg/kg
Chloromethane
Bromomethane
Vinyl Chloride
Dichlorodifluormethane
Chloroethane
Methylene Chloride
Trichlorofluormethane
1,1-Dichloroethylene
1,1-Dichloroethane
+-1,2-Dichloroethylene
Chloroform
1,2-Dichloroethane
1,1,1-Trichloroethane
Carbon Tetrachloride
Bromodichloromethane
1,2-Dichloropropane
+-1,3-Dichloropropene
Trichloroethylene
c-1,3-Dichloropropene
1,1,2-Trichloroethane
Chlorodibromomethane
2-Chloroethyl vinyl ether
Bromoform
1,1,2,2-Tetrachloroethylene
1,1,2,2-Tetrachloroet~~ne
Chlorobenzene
1,j-Dichlorobenzene
1,2-Dichlorobenzene
1,4-Dichlorobenzehe
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
30
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
!
SAMPLE I.D. MW-5 26.0-27.5
DATE ANALYZED 3ll8l86 BY Randall • VOLUME ANALYZED 2.0
COMPOUND CONCENTRATION
µg/kg
Chloromethane < 10
Bromomethane < 10
Vinyl Chloride < 10
Dichlorodifluormethane < 10
Chloroethane < 10
Methylene Chloride < 10
Trichlorofluormethane < 10
1,1-Dichloroethylene < 10
1,1-Dichloroethane < 10
+-1,2-Dichloroethylene < 10
Chloroform < 10
1,2-Dichloroethane < 10 • 1,1,1-Trichloroethane < 10
Carbon Tetrachloride < 10
Bromodichloromethane < 10
1,2-Dichloropropane < 10
+-1,3-Dichloropropene < 10
Trichloroethylene < 10
c-1,3-Dichloropropene < 10
1,1,2-Trichloroethane < 10
Chlorodibromomethane < 10
2-Chloroethyl vinyl ether ,,
< 10
Bromoform ·., < 10
l,l,2,2-Tetrachloroe2hylene < 10
1,1,2,2-Tetrachloroethane < 10 ;•l!·. Chlorobenzene < lO
l,3·Dichlorobenzene < 10
1,2-Dichlorobenzeri~ < 10
1,4-Dichlorobenzene < 10 • 1
SAMPLE I.D. ___ ~MW~-5=-~2=8~•=5~-3~0~-~0'------
DATE ANALYZED_~3~/=18=/~8~6~ ____ BY Randall •• VOLUME ANALYZED 2.0 -----=~~------
COMPOUND COIICENTRATIOII
µg/kg
Chloromethane < 10
Bromomethane < 10
Vinyl Chloride < 10
Dichlorodifluormethane < 10
Chloroethane < 10
Methylene Chloride < 10
Trichlorofluormethane < 10
1,1-Dichloroethylene < 10
1,1-Dichloroethane < 10
. , +-1,2-Dichloroethylene < 10
Chloroform < 10
l,2"Dichloroethane < 10
1,1,1-Trichloroethane < 10 • Carbon Tetrachloride < 10
Bromodichloromethane < 10
1,2-Dichloropropane < 10
+-1,3-Dichloropropene < 10
Trichloroethylene < 10
c-1,3-Dichloropropene < 10
1,1,2-Trichloroethane < 10
Chlorodibromomethane < 10
2-Chloroethyl vinyl ether ., < 10
Bromoform < 10 . t
1,1,2,2-Tetrachloroe~hylene < 10
1,1,2,2-Tetrachloroethane < 10
/t! Chlorobenzene < 10
1,3-Dichlorobenzene < 10
1,2-Dichlorobenzene < 10
1,4-Dichlorobenz~ne < 10 • •
SAMPLE I. D. ____ MW_-_5 __ 3_3_.-'-5_-3_4-','---4 ____ _
DATE ANALYZED_-"-3'--/l"-'8'-'/-"8-"-6 _____ BY Randall •• VOLUME ANALYZED 2.0 ----~-~-------
COMPOUND CONCENTRATION
µg/kg
Chloromethane < 10
Bre,momethane < 10
Vinyl Chloride < 10
Dichlorodifluormethane < 10
Chloroethane < 10
Methylene Chloride < 10
Trichlorofluormethane < 10
1,1-Dichloroethylene < 10
1,1-Dichloroethane < 10 . ,
+-1,2-Dichloroethylene < 10
Chloroform < 10
1,2-Dichloroethane < 10 • 1,1,1-Trichloroethane < 10
Carbon Tetrachloride < 10
Bromodichloromethane < 10
1,2-Dichloropropane < 10
+-1,3-Dichloropropene < 10
Trichloroethylene < 10
c-1,3-Dichloropropene < 10
1,1,2-Trichloroethane < 10
Chlorodibromomethane < 10 .,
2-Chloroethyl vinyl ether < 10
Bromoform ·., < 10 ·; 1,1,2,2-Tetrachloroethylene < 10
1,1,2,2-Tetrachloroet~fne < 10
Chlorobenzene < 10
1,3-Dichlorobenzene < 10
1, 2-Dichlorobenzen·~ < 10
1,4-Dichlorobenzene < 10 • <
SAMPLE I. D. ____ MW.cc.._-5"--_-"3-"8~-=-5--'3°"'8'--'"'-"9 ____ _
DATE ANALYZED._----"3,._/~18,:./c.:8ec6:_ ____ BY Randall
VOLUME ANALYZED 2.0 -------''-'-''-''-------
COMPOUND CONCENTRATION
µg/kg
Chloromethane < 10
Bromomethane < 10
Vinyl Chloride < 10
Dichlorodifluormethane < 10
Chloroethane < 10
Methylene Chloride < 10
Trichlorofluormethane < 10
1,1-Dichloroethylene < 10
1,1-Dichloroethane < 10
+-1,2-Dichloroethylene < 10
Chloroform < 10
1,2-Dichloroethane < 10 • 1,1,1-Trichloroethane < 10
Carbon Tetrachloride < 10
Bromodichloromethane < 10
1,2-Dichloropropane < 10
+-1,3-Dichloropropene < 10
Trichloroethylene < 10
c-1,3-Dichloropropene < 10
1,1,2-Trichloroethane < 10
Chlorodibromomethane < 10
2-Chloroethyl vinyl ether . ·,, < 10
Bromoform < 10 ·t
1, l, 2, 2-Tetrachloroed,ylene < 10
1,1,2,2-Tetrachloroethane < 10 .:~--Chlorobenzene < 10
1,3-Dichlorobenzene < 10
1,2-Dichlorobenzen~ < 10
1,4-Dichlorobenzepe < 10 • •
SAMPLE I.D. MW-5 43.5-43.8
DATE ANALYZED 3/18/86 BY Randall •• VOLUME ANALYZED 2.0
COMPOUND CONCENTRATION
µg/kg
Chloromethane < 10
Bromomethane < 10
Vinyl Chloride < 10
Dichlorodifluormethane < 10
Chloroethane < 10
Methylene Chloride < 10
Trichlorofluormethane < 10
1,1-Dichloroethylene < 10
1,1-Dichloroethane < 10
+-1,2-Dichloroethylene < 10
Chloroform < 10
1,2-Dichloroethane < 10
1,1,1-Trichloroethane < 10 • Carbon Tetrachloride < 10
Bromodichloromethane < 10
1,2-Dichloropropane < 10
+-1,3-Dichloropropene < 10
Trichloroethylene < 10
c-1,3-Dichloropropene < 10
1,1,2-Trichloroethane < 10
Chlorodibromomethane < 10
2-Chloroethyl vinyl ether . ···~ < 10
Bromoform < 10 .,
1,1,2,2-Tetrachloroethylene < 10
1,1,2,2-Tetrachloroethane < 10 /•~ Chlorobenzene < 10
l,3~Dichlorobenzene < 10
1,2-Dichlorobenzen~ < 10
1,4-Dichlorobenze~e < 10 • ·,
SAMPLE I. D •-----=-'MW"'---'5'-----"'53::c•:..,5:_-.::.5=.5;:..:. O:.._ ___ _
•• DATE ANALYZED 3/18/86 BY Randall -~===~----
VOLUME ANALYZED 2.0
COMPOUND CONCENTRATION
µg/kg
Chloromethane < 10
Bromomethane < 10
Vinyl Chloride < 10
Dichlorodifluormethane < 10
Chloroethane < 10
Methylene Chloride < 10
Trichlorofluormethane < 10
1,1-Dichloroethylene < 10
1,1-Dichloroethane < 10
+-1,2-Dichloroethylene < 10
Chloroform < 10
1,2-Dichloroethane < 10 • 1,1,1-Trichloroethane < 10
Carbon Tetrachloride < 10
Bromodichloromethane, < 10
1,2-Dichloropropane < 10
+-1,3-Dichloropropene < 10
Trichloroethylene < 10
c-1,3-Dichloropropene < 10
1,1,2-Trichloroethane < 10
Chlorodibromomethane < 10 .,
2-Chloroethyl vinyl ether < 10
Bromoform ·t < 10 ·, 1,1,2,2-Tetrachloroethylene < 10
1,1,2,2-Tetrachloroe~~ane < 10
Chlorobenzene < 10
1;3-Dichlorobenzene < 10
" 1,2-Dichlorobenzene < 10
• 1,4-Dichlorobenii!ne < 10
'
·-' 3/21/86 16:09:57
ACG STARTED
RUN: O: 1154609VOC
SCAN 1 OF 1300
, .PLE: 115-46-9 CMW-5 9: 05 3/21/86 AQUEOUS) SUBMITTED BY: 01
ANALYST: KING
COMMENTS: 5 ML SAMPLE DILUTED BY 5. CLP SURROGATE & INTERNAL STANDARDS ADDED AT 50 UG/L. FRIT SPARGER SYSTEM. GC PARAMETERS:
220 DEG= ZONE TEMP.
45 DEG= INITIAL TEMP.
220 DEG= FINAL TEMP.
3 MIN= INITIAL TIME
8.0 D/M = RAMP RATE
20 MIN= FINAL TIME
250 DEG= SEP. SET PT.
80 DEG= MANIF. SET PT.
INJ. MODE:PKD
0 SEC= DV OPN
FIL/MUL MODE:AUTO.
SCAN FROM 35 AMU TO 260 AMU IN 2.0 SEC.
3/21/86 16: 54:27
ACQUISITION COMPLETED
•
• '
•
100.0
RIC
56
• RIC
03/21/86 16:06:00
SAMPLE: 115-46-9 <MW-5 9:05 3✓21 ✓86 AQUEOUS)
200
6:50
400
13:40
516
607
600
20:30
685
DATA: 1154609UOC
753
800
27:20
914
1000
34:10
• SCANS 1 TO 1300
1209
1200
41:00
1595390.
SCAN
TIME
•
3.5
. ·., 65
1.8
128
100.0
130
250
8:32
• MASS CHROMATOGRAMS
03/21/86 16:06:00
•
SAMPLE: 115-46-9 <MW-5 9:05 3/21/86 AQUEOUS)
41~ • ".:f"':L.
2388'1.
300
5336.
31107.
300
10: 15
350
11:57
~S'Jt:.fi_
43737.
400
13: 40 .
DATA: 1154609UOC
450
15:22
• . .
SCANS 250 TO 540
516
5400.
26864 •
516
226304.
1154880.
500
17:05
I II
7968,
65.019
± 0.500
4168.
128.038
± 0.500
226304.
130.039
± 0.500
SCAN
TIME
4.8
92
59.9
98
62.5
114
100.0
164
550
18:47
•
.,
· MASS CHROMATOGRAMS
03/21/86 16:06:00
•
SAMPLE: 115-46-9 <MW-5 9:05 3/21/86 AQUEOUS)
. 607
200.
670.
: .. ··-
17248. -:i:.s
93841.
600
20:30
L
650
22:12
DATA: 1154609VOC
685
1776.
9704.
685
27616.
156745.
700
23:55
Cfi? .
7750.
1
16544.
95692.
-s.,..e. e. 2..
750
25:37
• SCANS 550 TO 790
1330.
92.028
± 0.500
16544.
98.029
± 0.500
17248.
114.034
± 0.500
27616.
164.049
± 0.500
SCAN
TIME
54.4
95
100.0
117
700
23:55
• MASS CHROMATOGRAMS
03/21/86 16:06:00
•
SAMPLE: 115-46-9 <MW-5 9:05 3✓21 ✓86 AQUEOUS)
753
12336. ::cs ,3
77229.
750
25:37
800
27:20
850
29:02
DATA: 1154609UOC
900
30:45
SCANS 700 TO 980
950
32:27
6712.
95.028
± 0.500
12336.
117.035
± 0.500
SCAH.
TIME
•
1022 r
SAMPLE
C2.H.CL3
M WT1~a •
3 PK 95 RANK 1 IN 3431 ,=IT 971
C5.H3.ci1.CL
M WT1f~a r
B PK 95 RANK 2 IN 3447 FIT 875 ·
C2.H.CL
,1 WT18ta r
B PK 60 RANK 3 IN 61 FIT 856
I I
I ,
M/E
• LIBRARY SEARCH
03/21/86 16:06:00 + 17:38 SAMPLE: 115-46-9 <MW-5 9:05 3/21/86 AQUEOUS) ENHANCED (S 15B 2N 0T)
ETHENE,TRICHLORO-
2H-PYRAN-1-~NE,6-CHLORO-
. ' ' . ' ' ETHYNE,CHLORO-
I I I I . . ' 40 60 80
DATA: 1154609VOC # 516
I
'
. ' .
100
.
I •
BASE M/E: 95
RIC: 1552380.
'
.
120
I
•
1022
SAMPLE
•
.,
,I
C2.CL4
n wT 1?~~ 3 PK 166 RAHK 1 IH 8119 FIT 998
•
C4.H5.02.CL3
n wT 1?g0 • B PK 96 RAHK 2 IH 11626 FIT 770
C. O. CL. F
.~ WT 18a~ •
B PK 47 RAHK 3 IN 333 FIT 756
.
...
.
40
•
LIBRARY SEARCH
03/21/86 16:06:00 + 23:24
SAMPLE: 115-46-9 (MW-5 9:05 3/21/86 AQUEOUS)
ENHANCED (5 15B 2H 0T)
I I I I.I ., . . . . ' ETHEHE,TETRACHLORO-
-~-
: .. -·--
I I , l1 I I . -. . PROPAHOICACI-D,2,2,3-TRICHLORO-
CARBOHICCHLORIDEFLUORIDE
60 80 100
DATA: 1154609VOC # 685
. .
I .
120 140
BASE M/E: 166
RIC: 232191.
I . .
" I . . .
160 180
r
1169
SAMPLE
C7 .H8 ..
11 WT 11§1
3 PK 91 RANK 1 IN 694 FIT 907
C7.H8
11 WT11§1 B PK 91 RANK 2 IN 697 FIT 885
C7.H10.N2
.'1 IH 1 rn1 B PK 91 RANK 3 rn 2610 FIT 884
•
40
• LIBRARY SEARCH
03/21/86 16:06:00 + 24:40
SAMPLE: 115-46-9 <MW-5 9:05 3/21/86 AQUEOUS)
ENHANCED (5 15B 2N 0T)
.. .-.:.,:
+c MS
-t-; me
50 60 70
DATA: BASE M/E: 91
RIC: 5151.
80 90 100 110 120