NCD003200383_19901010_Koppers Co. Inc._FRBCERCLA RA_Dioxin Furan Data Validation - CLP-OCR

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AWD
TICHNOLOGIES
PGH-90-TMJ-399
DATE October 10, 1990
TO Mr. Robert S. Markwell
Program Manager -Environmental Services
Beazer Materials and Services, Inc.
436 Seventh Avenue
Pittsburgh, Pennsylvania 15219
FROM Thomas M. Jackman
AWD Technologies, Inc.
SUBJECT Organic Data Validation -CLP
Keystone Environmental Job Nos. M90-06.04 and M90-06.22
overview
The set of samples for Beazer-Raleigh sampled 5/31/90 and 6/06/90
contained 22 samples. These included: 11 water samples including
4 rinsate blanks and 3 trip blanks and 11 soil samples including
1 pair of field duplicates. Samples were analyzed for Volatile
Organic Chemicals (VOAs), Semivolatiles (BNAs) and Pesticide/PCBs
by methods of the U.S. EPA's Contract Laboratory Program (CLP).
summary
All elements were successfully analyzed in all samples with the
exception of those qualified as unreliable, "R". Areas of concern
with respect to data usability are listed according to the
seriousness of the problem. These include:
Major Issues
Aqueous matrix spike/matrix spike duplicate
gamma-BHC (Lindane) were zero percent(O%).
result is qualified "J", biased very low
limits are qualified ''R'', unreliable.
(MS/MSD) recoveries for
Therefore a positive
and aqueous detection
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AWD Technologies, Inc.
PGH-90-TMJ-399
Mr. Roberts. Markwell
Beazer Materials and Services, Inc.
October 10, 1990 -Page 2
Minor Issues
Acetone, methylene chloride, bis(2-ethylhexyl) phthalate, alpha-
BHC and 4,4'-DDT were detected in field and/or laboratory blanks.
Positive results less than 10 times · the highest blank
concentrations of acetone, methylene chloride, bis(2-ethylhexyl)
phthalate and results less than 5 times the blank concentrations
of alpha-BHC and 4,4'-DDT are qualified ''U''.
The Percent Relative Standard Deviations (%RSDs) for 2-butanone and
benzyl alcohol exceeded the 30% quality control limit in initial
calibrations. Therefore detection limits of associated samples are
qualified "UJ", estimated.
The Percent Differences (%Os) for chloromethane, bromomethane,
carbon disulfide, vinyl acetate, 2-butanone, vinyl acetate,
bromoform, 2-hexanone, tetrachloroethane, benzyl alcohol,
2,4-dinitrophenol, 4-nitroaniline, 3,3'-dichlorobenzidine,
4-nitrophenol, dibenz(a,h)anthracene and benzo(g,h,i)perylene
exceeded quality control limits in continuing calibrations.
Therefore, detection limits of associated samples are qualified
''UJ'', estimated.
Notes
Positive results for acetone, methylene chloride, 4-methyl-2-
pentanone, 1,1,2,2-tetrachloroethane, dimethylphthalate,
2,4-dinitrophenol, pentachlorophenol, bis(2-ethylhexyl)phthalate,
naphthalene, 2-chlorophenol, phenanthrene, f luoranthene, pyrene,
alpha-BHC, 4,4'-DDT, methoxychlor, gamma-chlordane, dieldrin,
endrin and endosulfan I in some samples were reported at
concentrations below Contract Required Detect ion Limits. These
have been qualified ''J'' on the data summary.
Appendix B provides Tentatively
reported by the laboratory. TI Cs
contamination are crossed out and
Identified Results (TICs) as
which are the results of blank
initialed by the reviewer.
The data were reviewed according to the National Functional
Guidelines for Evaluating Organic Analyses. The text of this
report addresses only those problems affecting usability.
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AWD Technologies, Inc.
PGH-90-TMJ-399
Mr. Robert S. Markwell
Beazer Materials and Services, Inc.
October 10, 1990 -Page J
Information Regarding Report Content
Attachments:
1.
2 .
3.
4.
5.
Glossary of data qualifier codes.
Data Summary. This includes:
a) All positive results with qualifier codes, if applicable;
b) All unusable detection limits qualified with an "R"; and
c) All estimated detection limits qualified with UJ.
Appendix A -resu 1 ts as reported by the laboratory ( no
corrections were made during data validation).
Appendix B Tentatively Identified Compounds (TICs) as
reported by the laboratory with corrections made in data
validation.
Appendix C -Support Documentation includes details to support
the statement in this report.
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AWD Technologies, Inc.
GLOSSARY OF DATA QUALIFIER CODES (ORGANIC)
CODES RELATING TO IDENTIFICATION
(confidence concerning presence or absence of compounds)
U = Not Detected. The associated number indicates approximate
sample concentration necessary to be detected. Or, not
detected substantially above the level reported in laboratory
or field blanks.
(NO CODE) = Confirmed Identification
R = Unreliable Result. Analyte may or may not be present in the
sample. Supporting data necessary to confirm result.
CODES RELATED TO OUANTITATION
(can be used for positive results and sample quantitation limits):
J = Analyte present.
precise.
Reported value may not be accurate or
UJ = Not detected. Quantitation
imprecise.
OTHER CODES
NA= Not Analyzed
limit may be inaccurate or
I
I DA TA SUMMARY AQUEOUS VOLATILE RESULTS
lug/LI
I SAMPLES COLLECTED 5/31/90 ANO 6/06/90
KEYSTONE IORt OROER IM90·06.4 ANO IM90·06.22
I Saiple No. C·30·WA C·5 5A C·90A C·9IA
I COMPOUND
CHLOROMETHAME 10 U 23 ID U 24 I BROMOMETHANE 10 U 75 10 U 38
VINYL CHLORIDE IO U 10 U 10 U 10 U
CHLOROETHANE ID U 46 U 10 U 36 U
I METHYLENE CHLORIDE 11 U 28 U 5 U 7 U
ACETONE 11 U 10 U 27 16
CARBON DISULFIDE 5 U 5 U 5 U 5 UJ
I I, l·OICHLOROETHENE 5 U 30 5 U 31
I, l·OICHLOROETHANE 5 U 37 5 U 37
TOTAL l,2·0ICHLOROETHENE 5 U 5 U 5 U 5 U
I CHLOROFORM 5 U 38 5 U 41
I ,2·0ICHLOROETHANE 5 U 5 U 5 U 5 U
2·BUTANONE 10 UJ 10 U 10 U IO U
1, I, 1 · TRICHLOROETHANE 5 U 5 U 5 U 5 U
I CARBON TETRACHLORIDE 5 U 33 5 U 32
VINYL ACETATE 10 U 10 U 10 U 10 UJ
BROMOOICHLOROMETHANE 5 U 5 U 5 U 5 U
I I ,2·0ICHLOROPROPANE 5 U 35 5 U 37
CIH ,3·0ICHLOROPROPENE 5 U 5 U 5 U 5 U
TRICHLOROETHENE 5 U 36 5 U 37
I OIBROMOCHLOROMETHANE 5 U 5 U 5 U 5 U
I, 1, 2· TRICHLOROETHANE 5 U 36 5 U 45
BENZENE 5 U 5 U 5 U 5 U
TRANS·l,3·0ICHLOROPROPENE 5 U 5 U 5 U 5 U
I BROMOFORM 5 U 35 5 U 42 J
4·METHYL·2·PENTANONE 10 U 10 U 10 U IO U
2·HEXANONE IO U 10 U ID U IO UJ
I TETRACHLOROETHENE 5 U 5 U 5 U 5 U
1, 1, 2, 2· TETRACHLOROETHANE 5 U 32 5 U 42
TOLUENE 5 U 5 U 5 U 5 U
I CHLOROBENZENE 5 U 37 5 U 38
ETHYLBENZENE 5 U 5 U 5 U 5 U
STYRENE 5 U 5 U 5 U 5 U
TOTAL XYLENES 5 U 5 U 5 U 5 U I
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I DA TA SUMMARY AQUEOUS VOLATILE RESULTS
(ug/LI
I SAMPLES COLLECTED 5/31/90 AND 6/06/90
KEYSTONE IORK ORDER IM90_06.4 AND IM90_06.22
I Sa~ple No. S-R!NSATE TRIP iLANK TRIP BLANK TRIP BLANK X-RINSATE !-RINSATE !-R INSA TE
I COMPOUND
CHLOROMETHANE 10 U 10 UJ 10 U 10 U IO UJ 10 U IO U
I BROMOMETHANE ID U 10 UJ 10 U 10 U 10 UJ 10 U 10 U
VINYL CHLORIDE 10 U 10 U 10 U 10 U 10 U 10 U 10 U
CHLOROETHANE 10 U ID U 10 U 10 U 10 U 10 U IO U
METHYLENE CHLORIDE 8 5 U 12 13 4 6 5 U
I ACETONE IO U 21 15 10 U 8 9 ID U
CARBON DISULFIDE 5 U 5 UJ 5 U 5 U 5 UJ 5 UJ 5 U
I, 1-DICHLOROETHENE 5 U 5 U 5 U 5 U 5 U 5 U 5 U
I I, 1-DICHLOROETHANE 5 U 5 U 5 U 5 U 5 U 5 U 5 U
TOTAL 1,2-DICHLOROETHENE 5 U 5 U 5 U 5 U 5 U 5 U 5 U
CHLOROFORM 5 U 5 U 5 U 5 U 5 U 5 U 5 U
I I ,2-DICHLOROETHANE 5 U 5 U 5 U 5 U 5 U 5 U 5 U
2-BUTANONE 10 U 10 UJ 10 UJ IO UJ 10 UJ IO U 10 UJ
I, 1, I-TRICHLOROETHANE 5 U 5 U 5 U 5 U 5 U 5 U 5 U
CARBON TETRACHLORIDE 5 U 5 U 5 U 5 U 5 U 5 UJ 5 U
I VINYL ACETATE 10 U 10 U ID U 10 U 10 U IO U IO U
BROMOOICHLOROMETHANE 5 U 5 U 5 U 5 U 5 U 5 U 5 U
I, 2-DICHLOROPRO?ANE 5 U 5 U 5 U 5 U 5 U 5 U 5 U
I CIS-1 ,3-DICHLORDPROPENE 5 U 5 U 5 U 5 U 5 U 5 U 5 U
TR I CH LOROETHENE 5 U 5 U 5 U 5 U 5 U 5 U 5 U
DIBROMOCHLOROMETHANE 5 U 5 U 5 U 5 U 5 U 5 U 5 U
I I, I ,!-TRICHLOROETHANE 5 U 5 U 5 U 5 U 5 U 5 U 5 U
BENZENE 5 U 5 U 5 U 5 U 5 U 5 U 5 U
TRANS-I ,3-0!CHLDROPROPENE 5 U 5 U 5 U 5 U 5 U 5 U 5 U
BROMOFORM 5 U 5 U 5 U 5 U 5 U 5 UJ 5 U
I 4-METHYL-2-PENTANONE 4 10 U 10 U 10 U 10 U 10 U 10 U
2-HEXANONE 10 U 10 UJ 10 U 10 U 10 UJ 10 U IO U
TETRACHLOROETHENE 5 U 5 UJ 5 U 5 U 5 UJ 5 U 5 U
I 1, I ,2,2-TETRACHLOROETHANE 3 J 5 U 5 U 5 U 5 U 5 U 5 U
TOLUENE 5 U 5 U 5 U 5 U 5 U 5 U 5 U
CHLOROBENZENE 5 U 5 U 5 U 5 U 5 U 5 U 5 U
I ETHYLBENZENE 5 U 5 U 5 U 5 U 5 U 5 U 5 U
STYRENE 5 U 5 U 5 U 5 U 5 U 5 U 5 U
TOTAL XYLENES 5 U 5 U 5 U 5 U 5 U 5 U 5 U
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I DAT A SUMMARY SOIL VOLATILE RESULTS
lug/kg)
I SAMPLES COLLECTED 5/31/90 ANO 6/06/90
KEYSTONE WORK ORDER IM90_06.4 AND IM90_05.11
I Sample Ho. KOPPERS S-10-FB S-10-FB 5-10-FB S-t 3A-FB S-t3A-FB X-t-OSN
10-1) I 1-4 I I 2-4 ID I 0-1 I (1-4) (0-1)
I field Duplicates
CHLOROMETHANE t 1 U t 5 U 13 U 13 U t 3 U 13 U t 2 U
I BROMOMETHANE t 1 UJ 15 UJ t 3 UJ 13 UJ t 3 UJ t 3 UJ t 1 UJ
VINYL CHLORIDE 11 U 15 U t 3 U 13 U 13 U 13 U t 2 U
CHLOROETHANE 11 U 15 U 13 U t 3 U 13 U 13 U 12 U
METHYLENE CHLORIDE 13 U 43 U 16 U 14 U 16 U 1 t U 11 U
I ACETONE 16 U t 50 U t 60 U 110 U 82 U 47 U 15 U
CARBON DISULFIDE 10 8 U 6 U 6 U 6 U 6 U 6 UJ
t, t-DICHLOROETHENE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
I t, t-DICHLOROETHANE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
TOTAL t ,2-DICHLOROETHENE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
CHLOROFORM 6 U 8 U 6 U 6 U 6 U 6 U 6 U
I t ,2-DICHLOROETHANE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
1-BUTANONE 12 UJ 15 UJ t 3 UJ t 3 UJ 13 UJ 13 UJ t 2 U
t, 1, !-TRICHLOROETHANE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
CARBON TETRACHLORIDE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
I VINYL ACETATE 11 U 15 U 13 U 13 U 13 U ll U 12 U
BROMOOICHLOROMETHANE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
I ,2-DICHLOROPROPAHE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
I CIS-t,3-DICHLOROPROPENE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
TR I CHLOROE THE NE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
DIBROMOCHLOROMETHANE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
I t,1,2-TRICHLOROETHANE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
BENZENE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
TRANS-! ,3-DICHLOROPROPENE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
BROMOFORH 6 U 8 U 6 U 6 U 6 U 6 U 6 U
I 4-HETHYL-1-PENTAHONE 11 U 15 U 13 U 13 U 13 U 13 U 11 U
1-HEXANONE t 2 UJ t 5 UJ 13 UJ 13 UJ 13 UJ 13 UJ 11 UJ
TETRACHLOROETHENE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
I t ,1,1,1-TETRACHLOROETHANE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
TOLUENE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
CHLOROBENZEHE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
I ETHYLBENZENE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
STYRENE 6 U 8 U 6 U 6 U 6 U 6 U 6 U
TOTAL XYLENES 6 U 8 U 6 U 6 U 6 U 6 U 6 U
I Percent Moisture t 9 34 12 12 13 12 20
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I DA TA SUMMARY SOIL VOLATILE RESULTS
I ug/kg I
I SAMPLES COLLECTED 5/31/90 ANO 6/06/90
KEYSTONE WOR! ORDER IH90_06.4 IND IM90_06.22
I Sample No. X-39-EA X-46-WA l-7-LF X-93
I 0-2 I
I CHLOROMETHANE 12 U 15 UJ 13 UJ 13 U
I BROMOMETHANE 12 UJ 15 UJ 13 UJ 13 UJ
VINYL CHLORIDE 12 U 15 U 13 U 13 U
CHLOROETHANE 12 U 15 U 13 U 13 U
METHYLENE CHLORIDE 16 U 70 U 130 U 9 U
I ACETONE 10 U 12 U 680 U 20 U
CARBON DISULFIDE 6 U 8 U 6 U 6 UJ
1, 1-0ICHLOROETHENE 6 U 8 U 6 U 6 U
I 1, 1-0ICHLOROETHINE 6 U 8 U 6 U 6 U
TOTAL 1,2-0ICHLOROETHENE 6 U 8 U 6 U 6 U
CHLOROFORM 6 U 8 U 6 U 6 U
I 1,2-0ICHLOROETHANE 6 U 8 U I U 6 U
2-BUTANONE 12 UJ 15 UJ 13 UJ 13 U
1, 1, I-TRICHLOROETHANE 6 U 8 U 6 U 6 U
CARBON TETRACHLORIDE 6 U 8 U 6 U 6 U
I VINYL ACETATE 12 U 15 U 13 U 13 U
BROMOOICHLOROMETHANE 6 U 8 U 6 U 6 U
I ,2-0ICHLOROPROPANE 6 U 8 U 6 U 6 U
I CIS-1 ,3-0ICHLOROPROPENE 6 U 8 U 6 U 6 U
TRICHLOROETHENE 6 U 8 U 6 U 6 U
OIBROMOCHLOROHETHANE 6 U 8 U 6 U 6 U
I I, I ,2-TRICHLOROETHANE 6 U 8 U 6 U 6 U
BENZENE 6 U 8 U 6 U 6 U
TRANS-1 ,3-0!CHLOROPRDPENE 6 U 8 U 6 U 6 U
BROMOFORM 6 U 8 U 6 U 6 U
I 4-HETHYL-2-PENTANONE 12 U 15 U 13 U 13 U
2-HEXANONE 12 UJ I 5 UJ 13 UJ 13 UJ
TETRACHLOROETHENE 6 U 8 U 6 U 6 U
I I, 1,2,2-TETRICHLORDETHANE 6 U 8 U 6 U 6 U
TOLUENE 6 U 7 6 U 6 U
CHLOROBENZENE 6 U 8 U 6 U 6 U
I ETHYLBENZENE 6 U 8 U 6 U 6 U
STYRENE 6 U 8 U 6 U 6 U
TOTAL XYLENES 6 U 8 U 6 U 6 U
11 Percent Moisture 20 20 23 10
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I DA TA SUMMARY AQUEOUS SEMIVOLATILE RESULTS
I ug/1 I I SAMPLES COLLECTED 5/31/90 -6/06/90
!EYSTONE WORK ORDER IM90-06,04 ANO IM90-06.22
I Saflp1e No. C-90A C-9IA
I COMPOUND
I PHENOL 10 U 56
B1S12-CHLOROETHYL)ETHER 10 U 27
2-CHLOROPHENOL 10 U 52
I 1 ,3-DICHLOROBENZENE 10 U 10 U
1,4-0ICHLOROBENZENE 10 U 10 U
BENZYL ALCOHOL 10 UJ 10 UJ
1,2-0ICHLOROBENZENE 10 U 10 U
I 2-METHYLPHENOL 10 U 68
B!S12-CHLOROISOPROPYL)ETHER 10 U 10 U
4-METHYLPHENOL 10 U 10 U
I N-NITROSODI-N-PROPYLAMINE 10 U 10 U
HEXACHLOROETHANE 10 U 14
NITROBENZENE 10 U 10 U
I ISOPHORONE 10 U 30
2-NITROPHENOL 10 U IO U
2,4-0IMETHYLPHENOL 10 U 10 U
BENZOIC ACID 50 U 50 U I BISl2-CHLOROETHOXY)METHANE 10 U 10 U
2,4-DICHLORDPHENOL 10 U 10 U
1,2,4-TRICHLOROPHENOL 10 U 10 U
I NAPTHALENE 10 U 10 U
4-CHLROANILINE 10 U 10 U
HEXACHLOROBUTADIENE 10 U 10 U
I 4-CHLOR0-3-METHYPHENOL 10 U 10 U
2-METHYLNAPHTHALENE 10 U 10 U
HEXACHLOROCYCLOPENTADIENE 10 U 10 U
2,4,6-TRICHLOROPHENOL 10 U 10 U I 2,4,5-TRICHLOROPHENOL 50 U 50 U
2-CHLORONAPHTHALENE 10 U 10 U
2-NITROANILINE 50 U 50 U
I OIMETHYLPHTHALATE 10 U 2 J
ACENAPHTHYLENE 50 U 50 U
2,6-0INITROTOLUENE 10 U 10 U
I
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I OA H SUMMARY AQUEOUS SEMI10LATILE RESULTS
I uq/1 I
I SAMPLES COLLECTED 5/31/90 -6/06/90
KEYSTONE WORK ORDER IM90-06.04 ANO IM90-06.11
I Sample No. C-901 C-91A
I COMPOUND
I 3-NITROANILINE 50 U 50 U
ACENAPHTHENE 10 U 30
2,4-0INITROPHENOL 50 U 9 J
I 4-NITROPHENOL 50 U 50 U
OIBENZOFURAN 10 U 10 U
2,4-DINITROTOLUENE 10 U 10 U
OIETHYLPHTHALATE 10 U 10 U
I 4-CHLOROPHENYL-PHENYLETHER 10 U 10 U
FLUOR ENE 10 U 10 U
4-NITROAN!L!NE 50 U 50 U
I 4,6-0INITR0-2-METHYLPHENOL 50 U 50 U
N-NITROSOOIPHENYLAMINE 10 U 10 U
4-BROMOPHENYL·PHENYLETHER 10 U 10 U
I HEXACHLOROBENZENE 10 U 10 U
PENTACHLOROPHENOL 50 U 48 J
PHENANTHRENE 10 U 34
ANTHRACENE 10 U 10 U
I Dl·N·BUTYLPHTHALATE 10 U 10 U
FLUORANTHENE 10 U 10 U
PY RENE 10 U 30
I BUTYLBENZYLPHTHALATE 10 U 10 U
3,3'·0ICHLOROBENZIDINE 20 UJ 10 UJ
BENZOIA)ANTHRACENE 10 U 10 U
I CHRYSENE 10 U 10 U
B!S12-ETHYLHEXYL)PHTHALATE 3 U 3 U
Ol·N·OCTYLPHTHALATE 10 U 10 U
BENZOIB)FLUORANTHENE 10 U 18
I BENZOIK)FLUORANTHENE 10 U 10 U
BENZOI A )PYRENE 10 U 10 U
INOENOl1,2,3·CO)PYRENE 10 U 10 U
.1 OIBENZIA,H)ANTHRACENE 10 U 10 U
BENZOIG,H,l)PERYLENE 10 U 19
1,
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I DATA SUMMARY AQUEOUS SEM!iOLAT!LE RESULTS
I ug/1 I
I SAMPLES COLLECTED 5/31/90 · 6/06/90
KEYSTONE WORK ORDER IM90-06.04 ANO IM90-06.11
I Sample No. S·RINSATE X-RJNSATE X·RJNSATE X·RJNSATE
I COMPOUND
I PHENOL 10 U 10 U IO U 10 U
8JSl1-CHLOROETHYLIETHER 10 U 10 U 10 U 10 U
2-CHLOROPHENOL 10 U 10 U 10 U 10 U
1,3-0JCHLOROBENZENE 10 U 10 U 10 U 10 U I 1 ,4-0ICHLOROBENZENE 10 U 10 U 10 U 10 U
BENZYL ALCOHOL 10 UJ 10 UJ 1 D UJ 10 UJ
I ,1-0ICHLOROBENZENE 10 U 10 U 10 U 10 U
I 1-METHYLPHENOL 10 U IO U 10 U 10 U
8JS(1-CHLOROJSOPROPYL)ETHER 10 U 10 U 10 U 10 U
4-METHYLPHENOL 10 U 10 U 10 U 10 U
I N-NJTROSOOJ-N-PROPYLANINE 10 U 10 U 10 U 10 U
HEXACHLOROETHANE 10 U 10 U 10 U IO U
NJTROBENZENE 10 U 10 U 10 U 10 U
JSOPHORONE 10 U IO U 10 U 10 U
I 1-NJTROPHENOL 10 U IO U 10 U 10 U
1,4-0INETHYLPHENOL 10 U 10 U 10 U 10 U
BENZOIC ACID 50 U 50 U 50 U 50 U
I 81Sl2-CHLOROETHOXY)NETHANE 10 U IO U 10 U 10 U
2,1-0ICHLOROPHENOL 10 U 10 U 10 U 10 U
I ,1,4-TRJCHLOROPHENOL 10 U 10 U 10 U 10 U
I NAPTHALEHE 10 U 10 U 10 U 10 U
4-CHLROANILINE 10 U 10 U 10 U 10 U
HEXACHLOROBUTADIENE 10 U 10 U 10 U 10 U
4-CHLOR0-3-METHYPHENOL 10 U 10 U 10 U 10 U
I 1-METHYLNAPHTHALENE 10 U 10 U 10 U 10 U
HEXACHLOROCYCLOPENTADJENE 10 U 10 U 10 U 10 U
2,1,6-TRJCHLOROPHENOL 10 U 10 U 10 U 10 U
I 2,4,5-TRJCHLOROPHENOL 50 U 50 U 50 U 50 U
1-CHLORONAPHTHALENE 10 U 10 U 10 U 10 U
1-NITROANILINE 50 U 50 U 50 U 50 U
I OJMETHYLPHTHALATE 10 U 10 U 10 U 10 U
ACENAPHTHYLENE 50 U 50 U 50 U 50 U
2,6-0IHJTROTOLUENE 10 U 10 U 10 U 10 U
I
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I DA TA SUMMARY AQUEOUS SEMIVOLATILE RESULTS
I ug/1 I
I SAMPLES COLLECTED 5/31/90 · 6/06/90
KEYSTONE IORK ORDER IM90-06.04 AND IM90·06.11
I S1~ple Ne. S-RINSATE X·RINSATE X-RINSATE X·R!NSATE
I COMPOUND
I 3-NITROANILINE 50 U 50 U 50 U 50 U
ACENAPHTHENE 50 U 50 U 50 U 50 U
2.4-0INITROPHENOL 10 U 10 U 10 U 10 U
4-NITROPHENOL 10 UJ 10 U 10 U 10 U I DIBENZOFURAN 10 U 10 U 10 U 10 U
1,4-DINITROTOLUENE 10 U 10 U 10 U IO U
DIETHYLPHTHALATE 10 U 10 U 10 U 10 U
I 4-CHLOROPHENYL·PHENYLETHER 10 U 10 U 10 U 10 U
FLUORENE IO U 10 U 10 U IO U
4-NITROANILINE 50 U 50 U 50 U 50 U
I l,6-0INITR0-1-METHYLPHENOL 50 U 50 U 50 U 50 U
N-N!TROSOOIPHENYLAMINE 10 U 10 U 10 U 10 U
4-BROMOPHENYL·PHENYLETHER 10 U 10 U 10 U 10 U
HEXACHLOROBENZENE 10 U 10 U 10 U 10 U
I PENTACHLOROPHENOL 50 U 50 U 50 U 50 U
PHENANTHRENE 10 U 10 U 10 U 10 U
ANTHRACENE 10 U 10 U 10 U 10 U
I Dl·N·BUTYLPHTHALATE 10 U 10 U 10 U 10 U
FLUORANTHENE 10 U 10 U 10 U 10 U
PYRENE 10 U 10 U 10 U 10 U
I BUTYLBENZYLPHTHALATE 10 U 10 U 10 U 10 U
3.J'·OICHLOROBENZIDINE 10 U 10 UJ 10 UJ 10 UJ
BENZOIA)ANTHRACENE 10 U 10 U 10 U 10 U
CHRYSENE 10 U 10 U 10 U 10 U
I BIS(1-ETHYLHEXYL)PHTHALATE 1 10 U 11 1
O1-N-OCTYLPHTHALATE 10 U 10 U 10 U 10 U
BENZOIB)FLUORANTHENE 10 U 10 U 10 U IO U
I BENZO(K)FLUORANTHENE 10 U IO U 10 U 10 U
BENZOIA)PYRENE 10 U 10 U 10 U 10 U
INOEN0(1,1,3-CD)PYREME 10 U 10 U 10 U 10 U
I OIBEMZIA,H)ANTHRACENE 10 U 10 U 10 U 10 U
BEMZOIG,H,l)PERYLENE 10 U 10 U 10 U 10 U
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I DA TA SUMMARY SOIL SEMIYOLATILE RESULTS
lug/kg)
I SAMPLES COLLECTED 5/31/90 -6/06/90
KEYSTONE WORK ORDER IM90-06.0I AND IM90-06.22
I Saflple No. S-10-FB S-10-FB S-10-FB 5-13-FB S-13-FB
I 0-2' I I 1-4' I 11-1' ID I 0-1' I I 2-1' I
I COMPOUND
PHENOL 500 U 110 U 120 U 130 U 110 U
I B!S12-CHLOROETHYL)ETHER 500 U 410 U 110 U 130 U 110 U
2-CHLOROPHENOL 500 U 120 U 110 U 130 U 110 U
I ,3-DICHLOROBENZENE 500 U 110 U 110 U 130 U 120 U
1,1-DICHLOROBENZENE 500 U 410 U 120 U 430 U 410 U
I BENZYL ALCOHOL 500 UJ 410 UJ 110 UJ 130 UJ 120 UJ
1.2-0ICHLOROBENZENE 500 U 110 U 120 U 130 U 120 U
2-METHYLPHENOL 500 U 110 U 410 U 430 U 120 U
I 81512-CHLOROISOPROPYL)ETHER 500 U 120 U 120 U 130 U 120 U
4-METHYLPHENOL 500 U 110 U 110 U 130 U 120 U
N-NITROSOD!-N-PROPYLAMINE 500 U 420 U 420 U 430 U 420 U
I HEXACHLOROETHANE 500 U 120 U 420 U 430 U 420 U
N!TROBENZENE 500 U 420 U 410 U 130 U 420 U
ISOPHORONE 500 U 420 U 410 U 130 U 420 U
1-N!TROPHENOL 500 U 120 U 420 U 430 U 420 U
I 1,1-DIMETHYLPHENOL 500 U 420 U 410 U 430 U 420 U
BENZOIC ACID 2100 U 1100 U 1100 U 2100 U 1100 U
815(2-CHLOROETHOXY)METHANE 500 U 420 U 120 U 430 U 420 U
I 1,1-D!CHLOROPHENOL 500 U 120 U 110 U 130 U 110 U
1,1,4-TR!CHLOROPHENOL 500 U 420 U 410 U 130 U 110 U
NAPTHALENE 500 U 110 U 110 U 430 U 420 U
I 1-CHLROAN!l!NE 500 U 120 U 110 U 430 U 420 U
HEXACHLOROBUTADIENE 500 U 110 U 110 U 130 U 120 U
I-CHLOR0-3-METHYPHENOL 500 U 410 U 110 U 130 U 120 U
1-METHYLNAPHTHALENE 500 U 420 U 110 U 130 U 110 U
I HEXACHLOROCYCLOPENTADIENE 500 U 110 U 120 U 130 U 110 U
2,1,6-TR!CHLOROPHENOL 500 U 420 U 120 U 430 U 110 U
2,4,5-TRICHLOROPHENOL 2400 U 2100 U 2100 U 2100 U 2100 U
I 2-CHLORONAPHTHALENE 500 U 410 U 420 U 130 U 420 U
2-NITROANILIME 2400 U 2100 U 2100 U 2100 U 2100 U
DIEMTHYLPHTHALATE 500 U 420 U 420 U 430 U 420 U
I ACENAPHTHYLENE 500 U 420 U 120 U 430 U 120 U
2,6-DINITROTOLUENE 500 U 420 U 420 U 430 U 420 U
PERCENT MOISTURE 34 22 22 23 22
I
I
I
I
I
I OA Tl SUMMARY SOIL SEMIVOLAT!LE RESULTS
(ug/kg)
I SAMPLES COLLECTED 5/31/90 -6/06/90
KEYSTONE WORK ORDER IM90-06.04 ANO IM90-06.22
I Sanple No. S-10-fB S-10-fB S-10-fB S-13-fB S-13-fB
I 0-2' I I 2-4' I I 2-4' ID I 0-2' I IH'I
I COMPOUND
3-NITROANlllNE 2400 U 2100 U 2100 U 2100 U 2100 U
I ACENAPHTHENE 500 U 420 U 420 U 430 U 420 U
2,4-0INITROPHENOL 2400 UJ 2100 UJ 2100 UJ 2100 U 2100 U
4-NITROPHENOL 2400 U 2100 U 2100 U 2100 U 2100 U
DIBENZOfURAN 500 U 420 U 420 U 430 U 420 U
I 2,4-DIN!TROTOLUENE 500 U 420 U 420 U 430 U 420 U
DIETHYLPHTHALATE 500 U 420 U 420 U 430 U 420 U
4-CHLOROPHENYL-PHENYLETHER 500 U 420 U 420 U 430 U 420 U
I fLUORENE 500 U 420 U 420 U 430 U 420 U
4-NITROANILINE 2400 UJ 2100 UJ 2100 UJ 2100 UJ 2100 U
4,6-D!N!TR0-2-METHYLPHENOL 2400 U 2100 U 2100 U 2100 U 2100 U
I N-NITROSOOIPHENYLAMINE 500 U 420 U 420 U 430 U 420 U
4-BROMOPHENYL-PHENYLETHER 500 U 420 U 420 U 430 U 420 U
HEXACHLOROBENZENE 500 U 420 U 420 U 430 U 420 U
PENTACHLOROPHENOL 2400 U 2100 U 2100 U 2100 U 2100 U
I PHENANTHRENE 500 U 420 U 420 U 430 U 420 U
ANTHRACENE 500 U 420 U 420 U 430 U 420 U
01-N-BUTYLPHTHALATE 500 U 420 U 420 U 430 U mu
I fLUORANTHENE 500 U 420 U 420 U 430 U 420 U
PYRENE 500 U 420 U 420 U 430 U 420 U
BUTYLBENZYLPHTHALATE 500 U 420 U 420 U 430 U 420 U
I 3,3'-0ICHLOROBENZID!NE I 000 U 850 U 850 U 860 U 850 UJ
BENZO(AIANTHRACENE 500 U 420 U 420 U 430 U 420 U
CHRYSENE 500 U 420 U 420 U 430 U 420 U
BIS(2-ETHYLHEXYL)PHTHALATE 100 U 420 U 420 U 430 U 420 U
I 01-N-OCTYLPHTHALATE 500 U 420 U 420 U 430 U 420 U
BENZO(B)fLUORANTHENE 500 U 420 U 420 U 430 U 420 U
BENZO(K)fLUORANTHENE 500 U 420 U 420 U 430 U 420 U
I BENZO(A)PYRENE 500 U 420 U 420 U 430 U 420 U
I NOE NO I 1 , 2, 3-CO I PYRENE 500 U 420 U 420 U 430 U 420 U
OIBENZ(A,H)ANTHRACENE 500 U 420 U 420 U 430 UJ 420 U
I BENZO(G,H,I)PERYLENE 500 U 420 U 420 U 430 UJ 420 U
PERCENT MOISTURE 34 22 22 23 22
I
I
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I
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I DA TA SUMMARY SOIL SEMIYOLATILE RESULTS
I SAMPLES COLLECTED 5/31/90 -6/06/90
lug/kg)
KEYSTONE -ORK OROER IM90-06.04 ANO IM90-06.22
I Suple No. S-80 H-OSN X-39-EA X-46--A X-7-lf X-93 X-94
I 0-2' I I 0-2' I
I COMPOUND
PHENOL 1900 410 U 410 U 820 U 430 U 310 U 1100 I BISl2-CHLOROETHYL)ETHER 310 U 410 U 410 U 820 U 430 U 310 U 360 U
2-CHLOROPHENOL 820 410 U 410 U 820 U 430 U 310 U 200 J
1 ,3-DICHLOROBENZENE 310 U 410 U 410 U 820 U 430 U 370 U 360 U
• 1,4-DICHLOROBENZENE 370 U 410 U 410 U 820 U 430 U 370 U 360 U
BENZYL ALCOHOL 370 UJ 410 UJ 410 UJ 820 UJ 430 UJ 310 UJ 360 UJ
1,2-0ICHLOROBENZENE 3 70 U 410 U 410 U 820 U 4 30 U 310 U 360 U I 2-METHYLPHENOL 1900 410 U 410 U 820 U 430 U 310 U 1300
BISl2-CHLOROISOPROPYL)ETHER 310 U 410 U 410 U 820 U 430 U 370 U 360 U
4-METHYLPHENOL 310 U 410 U 410 U 820 U 430 U 310 U J60 U I N-NITROSODI-N-PROPYLAMINE 310 U 410 U 410 U 820 U 430 U 370 U 360 U
HEXACHLOROETHANE 310 U 410 U 410 U 820 U 430 U 310 U 360 U
NITROBENZENE 310 U 410 U 410 U 820 U 430 U 310 U 360 U
ISOPHORONE 680 410 U 410 U 820 U 430 U 310 U 430
12-NITROPHENOL 310 U 410 U 410 U 820 U 430 U 310 U 360 U
2,4-DIMETHYLPHENOL 310 U 410 U 410 U 820 U 430 U 370 U 360 U
BENZOIC ACID 1800 U 2000 U 2000 U 4000 U 2100 U 1800 U 1100 U I BISI 2-CHLOROETHOXY )METHANE 310 U 410 U 410 U 820 U 430 U 370 U 360 U
2,4-DICHLOROPHENOL 370 U 410 U 410 U 820 U mu 310 U 350 U
1,2,4-TRICHLOROPHENOL 370 U 410 U 410 U 820 U 430 U 3 70 U 360 U
NAPTHALENE 310 U 410 U 58 J 820 U 430 U 370 U 360 U
14-CHLROAN!l!NE 370 U 410 U 410 U 820 U 430 U 310 U 350 U
HEXACHLOROBUTADIENE 370 U 410 U 410 U 820 U 430 U 310 U 350 U
4-CHLOR0-3-METHYPHENOL 310U 410 U 410 U 820 U 430 U 3 70 U 350 U I 2-METHYLNAPHTHALENE 310 U 410 U 410 U 820 U 430 U 310 U 360 U
HEXACHLOROCYCLOPENTADIENE 310 U 410 U 410 U 820 U 430 U 370 U 360 U
2,4,8-TRICHLOROPHENOL 310 U 410 U 410 U 820 U 430 U 310 U 360 U I 2,4,5-TRICHLOROPHENOL 1800 U 2000 U 2000 U 4000 U 2100 U 1800 U 1700 U
2-CHLORONAPHTHALENE 310U 410 U 410 U 820 U 430 U 370 U 350 U
2-NITROANILINE 1800 U 2000 U 2000 U 4000 U 2100 U 1800 U 1100 U I DIENTHYLPHTHALATE 1200 410 U 410 U 820 U 430 U 370 U 1000
ACENAPHTHYLENE 310 U 410 U 410 U 820 U 430 U 310 U 350 U
2,5-0INITROTOLUENE 310 U 410 U 410 U 820 U 430 U 310 U 350 U
I PERCENT MOISTURE 10 20 20 20 23 10 8
I
I
I
I I OAT I SUMMARY SOIL SEMIYOLATILE RESULTS SAMPLES COLLECTED 5/31/90 · 6/06/90 I (ug/kgl I KEYSTONE WORK ORDER IN90·06.04 ANO IN90-06.11 I Sample No. S-80 X-1-0SN X-39-EI X-46-WA X-7-LF 1-93 1-94 I 0-2' I I 0-1' I I COMPOUND 3-NITR0ANILINE 1800 U 1000 U 1000 U 4000 U 2100 U 1800 U 1700 U ACENAPHTHENE 800 410 U 410 U 820 U 430 U 370 U 540 I 2,4-0INITROPHENOL 750 J 1000 U 1000 U 4000 UJ 1100 U 1800 UJ 1400 J 4-NITROPHENOL 1800 U 1000 U 1000 U 4000 U 2100 UJ 1800 U 1700 UJ OI8ENZOFURAN 310 U 410 U 410 U 810 U 430 U 370 U 360 U I 1,4-0INITROTOLUENE 370 U 410 U 410 U 810 U 430 U 370 U 360 U OIETHYLPHTHILATE 3 70 U 410 U 410 U 810 U 430 U 370 U 360 U 4-CHLOROPHENYL-PHENYLETHER 370 U 410 U 410 U 810 U 430 U 370 U 360 U I FLUORENE 370 U 410 U 410 U 820 U 430 U 370 U 360 U 4-NITR0ANILINE 1800 U 1000 U 2000 U 4000 UJ 1100 U 1800 UJ 1700 U 4.6-DINITR0-1-METHYLPHENOL 1800 U 1000 U 1000 U 4000 U 1100 U 1800 U 1700 U N-NITROSOOIPHENYLAMINE 370 U 410 U 410 U 810 U 430 U 370 U 360 U I 4-BROMOPHENYL-PHENYLETHER 370 U 410 U 410 U 810 U 430 U 370 U 360 U HEXACHLOROBENZENE 370 U 410 U 410 U 810 U 430 U 370 U 360 U PENTACHLOROPHENOL 1500 1000 U 460 J 4000 U 1100 U 1800 U 1300 J I PHENANTHRENE 1400 410 U 91 J 820 U 430 U 370 U 990 INTHRACENE 370 U 410 U 410 U 820 U 430 U 370 U 360 U OI-N-8UTYLPHTHALATE 370 U 410 U 410 U 810 U 430 U 370 U 360 U I FLUORINTHENE 3 70 U 410 U 110 J 820 U 430 U 370 U 360 U PYRENE 1600 410 U 94 J 810 U 430 U 370 U 1100 BUTYL8ENZYLPHiHALITE 370 U 410 U 410 U 810 U 430 U 370 U 360 U I 3,3'·0ICHLOR08ENZIOINE 730 U 810 UJ 810 UJ 1600 U 860 U ; 30 U 7 30 U 8ENZ0IA)ANTHRACENE 370 U 410 U 410 U 810 U 430 U 370 U 360 U CHRYSENE 370 U 410 U 410 U 810 U 430 U 370 U 360 U BISl1-ETHYLHEXYL)PHTHALATE 100 U 2500 U 130 U 1100 U 1000 U 74 U 360 U I DI-N-OCTYLPHTHALATE 370 U 410 U 410 U 810 U 430 U 370 U 360 U BENZ0(8)FLUORINTHENE 1600 410 U 410 U 810 U 430 U 370 U 1100 8ENZO(K)FLUORANTHENE 370 U 410 U 410 U 810 U 430 U · 370 U 360 U I 8ENZO(A)PYRENE 370 U 410 U 410 U 810 U 430 U 370 U 360 U INDENO( 1 ,1,3-CD)PYRENE 370 U 410 U 410 U 810 U 430 U 370 U 360 U DI8ENZIA,H)ANTHRACENE 370 U 410 U 410 U 810 U 430 U 370 U 360 U I 8ENZOIG,H,I)PERYLENE 1400 410 U 410 U 810 U 430 U 370 U 960 PERCENT MOISTURE 10 I 10 20 20 23 10 I I :I I 11 I
I
I OH I SUMMARY AQUEOUS PES ICIDE/PCB RESULTS
I ug/ LI
I SAMPLES COLLECTED 5/31/90 • 6/06/90
KEYSTONE •ORK ORDER IM90-06.04 ANO IM90·06.22
I Sa~ple No. C-90A C-91A
I
I ALPHA·BHC 0.050 U 0.55 ' BETA·BHC 0.050 U 0. 05 U
OELTA-BHC 0.050 U 0 .05 U
I GAMMA-BHC (LINOANE) o.o5o R 0.064 J ' HEPTACHLOR 0. 050 U 0.40
ALDRIN 0.050 U 0 .05 U
I HEPTACHLOR EPOXIOE 0.050 U 0. 05 U ' ENOOSULFAN I 0.10 U 0. 05 U ' OIELORIN 0. 10 U 0.88 '
I 4,4'-00E 0.10 U
1 1.0 U
ENDRIN 0. 10 U 1.0 U
EMOOSULFAN II 0. 10 U 0.76
4,4'-000 0. 10 U 1.0 U
I EMOOSULFAN SULFITE 0. 10 U 1.0 U
4,4'-00T 0. 10 U 0.59
METHOXYCHLOR 0. 50 U 5.0 U
I ENORIN KETONE 0. 10 U 1.0 U
ILPHA·CHLOROANE 0.50 U 5 .0 U
GAMMI-CHLOROINE 0. 50 U 5.0 U
I TOXAPHENE 1.0 U 10 U
IROCLOR-1016 0. 50 U 5.0 U
AROCLOR-1221 0.50 U 5.0 U
AROCLOR-1232 0. 50 U 5.0 U
I IROCLOR-1242 0. 50 U 5.0 U
IROCLOR-1248 0.50 U 5.0 U
IROCLOR-1254 1.0 U 10 U
I IROCLOR-1260 1.0 U 10 U
I
I
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I
D
I DATA SUMMARY AQUEOUS PESTICIDE/PCB RESULTS
I ug/ LI
I SAMPLES COLLECTED 5/31/90 -6/06/90
KEYSTONE •ORK ORDER IM90-06.0I AND IM90-06.22
I Sample No. X-RINSATE X-RINSATE X-RINSATE S-RINSA TE
I
I ALPHA-BHC 0.050 U 0.0019 J 0.050 U 0.050 U
BETA-BHC 0.050 U 0.050 U 0.050 U 0.050 U
DE LT A-BHC 0.050 U 0.050 U 0.050 U 0.050 U
I GAMMA-BHC 1. LIN DANE I 0. 050 R 0.050 R 0.050 R 0.050 R
HEPTACHLOR 0.050 U 0.050 U 0.050 U 0.050 U
ALDRIN 0. 050 U 0.050 U 0.050 U 0.050 U
I HEPTACHLOR EPOXIDE 0. 0 50 U 0.050 U 0.050 U 0.050 U
ENDOSULFAN I 0. 10 U 0. IO U 0. 10 U 0. 10 U
DIELDRIN 0. 10 U 0. 10 U 0. 10 U 0. 10 U
I 1,1'-DDE 0, 10 U 0. 10 U 0, 10 U 0. IO U
ENDRIN 0. 10 U 0. 10 U 0. 10 U 0. IO U
ENDOSULFAN I I 0. IO U 0.10 U 0. 10 U 0 .10 U
4,1'-DDD 0. IO U 0.10 U 0. 10 U 0. 10 U
I ENDOSULFAN SULFATE 0. IO U 0 .10 U 0.10 U 0. 10 U
1,1'-DDT 0.020 J 0.10 U 0. 10 U 0. IO U
METHOXYCHLOR 0.50 U 0.50 U 0. 50 U 0. 50 U
I ENDRIN KETONE D, 10 U 0.10 U D. ID U 0. 10 U
ALPHA-CHLORDANE 0.50 U 0.50 U 0. 50 U 0.50 U
GAMMA-CHLORDANE 0. 50 U 0. 50 U D. 50 U 0. 50 U
I TOXAPHENE 1.0 U 1.0 U 1.0 U 1.0 U
AROCLOR-1016 D. 50 U 0. 50 U 0. 50 U 0.50 U
AROCLOR-1221 0.50 U 0.50 U 0.50 U 0.50 U
AROCLOR-1232 o. 50 lu 0. 50 U 0. 50 U 0.50 U
I AROCLOR-1242 0. 50 U 0.50 U 0.50 U 0. 50 U
AROCLOR-1248 0.50 U 0.50 U 0. 50 U 0. 50 U ' AROCLOR-1254 1.0 U ' 1.0 U 1.0 U 1.0 U
I AROCLOR-1260 1.0 U 1.0 U 1.0 U 1.0 U I
I
I
I
I
I
I g 01 TA SUMMARY I SOIL PESTICIDE/PCB RESULTS lug/kg) n SIMPLES COLLECTED 5/31/90 -6/06/90 KEYSTONE •ORK ORDER IM90-06.0I IND IM90r6.11 D S1~ple No. S-10-FB S-10-FB S-10-FB S-13-FB 5-13-FB 5-13-FB I 0-1' I I 1-1' I I 2-4' ID I 0-1' I I 1-4' I I 2-1' I I Field Duplicates l Field Duplicates I ILPHI-BHC 12 u 10 U 10 U 10 U 3.0 U 10 U BETI-BHC 12 u 10 U 10 U 10 U 13 10 U OELTI-BHC 12 u 10 U 10 U 10 U 10 U 10 U I GIMMI-BHC (L!NDINE) 12 u 10 U 10 U 10 U 10 U 10 U HEPTICHLOR 12 u 0. 11 10 U 10 U 10 U 10 U ' ALDRIN 12 U 10 U 10 U 10 U 10 U 10 U I HEPTICHLOR EPOXIOE ,i u 10 U 10 U 10 U 10 U 10 U ENOOSULFAN I ,i u 10 U 10 U 10 U 10 U 10 U OIELDRIN 24 u 21 U 21 U 21 U 11 U 1.6 J 4,1'-DOE ' I 14 U 11 U 11 U 11 U 21 U 20 U ' ENOR!N 24 U 21 U 11 U 11 U 21 U 20 U ' 11 U 21 U 14 J 20 U ENOOSULFIN 11 14 U 21 U ' 1,4'-0DD 14, U 21 U 11 U 21 U 11 U 20 U I ENDOSULFIN SULFITE 14, U 11 U 21 U 11 U 21 U 10 U 4,4'-001 : 2~; ~ 11 U 21 U 11 U 1.8 u 0. 71 U METHOXYCHLOR 100 U 100 U 100 U 18 J 18 J I ENDRIN KETONE 24 U 21 U 21 U 21 U 11 U 10 U A LPHI-CHLOROANE 120 U 100 U 100 U 100 U 100 U 100 U GAMMA-CHLORDANE 110 U 100 U 100 U 100 U 1.6 J 100 U I TOXIPHENE 140 U 110 U 110 U 210 U 110 U 200 U IROCLOR-1016 120 U 100 U 100 U 100 U 100 U 100 U AROCLOR-1221 120 U 100 U 100 U 100 U 100 U 100 U AROCLOR-1232 120 U 100 U 100 U 100 U 100 U 100 U I IROCLOR-1242 120 U 100 U 100 U 100 U 100 U 100 U AROCLOR-1248 110 U 100 U 100 U 100 U 100 U 100 U IROCLOR-1254 140 U 210 U 210 U 110 U 210 U 100 U I IROCLOR-1160 240 U 210 U 210 U 210 U 210 U 200 U PERCENT MOISTURE 34 I 21 21 23 21 10 I I I I I
g D DH A SUMMARY I SOIL PESTICIDE/PCB RESULTS lug/kg I n SAMPLES COLLECTED 5/31/90 · 6/08/90 !EYSTONE WORK ORDER IM90-06.0l ANO IM90-06.11 B I Sample No. S-80 l-l·OSN l-93 X-H l-46-WA X-7-LF I I 0·1' I n D ALPHA-BHC 1·, 10 U 8.9 U 11 10 U 10 U I BETA-BHC 8.9 U 10 U 8.9 U 8. 7 U 10 U 13 U ' OELTA·BHC 8.9 U 10 U 8.9 U 8. 7 U 10 U 10 U D GAMMA·BHC (LINOANEI 8 .9 U ! 0 U 8. 9 U 8. 7 U 10 U 10 U HEPTACHLOR 32 10 U 8.9 U 11 10 U 10 U ALDRIN 8. 9 u 10 U 8. 9 U 8. 7 U 10 U 0.29 U ' HEPTACHLOR EPO!IOE D 8.9 U 10 U 8.9 U 8. 7 U 10 U 10 U ENOOSULFAN I 8 .9 U 10 U 8.9 U 8. 7 U 0.3' J 10 U DIE LORIN 28 20 U 18 U 17 20 U 21 U I l,l'-OOE 18 u 20 U 18 U 17 U 20 U 11 U ENORIN 18 u 20 U 18 U 17 U UJ 21 J ' ENOOSULFAN II 38 10 U 18 U 21 U 20 U 11 U ,,,·-ooo 18 u 10 U 18 U 17 U 10 U 21 U R ENOOSULFAN SULFATE 18 u 10 U 18 U 17 U 20 U 21 U l,l'·OOT 38 20 U 18 J 21 3.2 U 0.92 U METHOXYCHLOR 89 u 100 U 89 U 87 U 100 U 100 U I ENORIN KETONE 18 u 20 U 18 U 17 U 20 U 21 U ALPHA-CHLORDANE 89 u 100 U 89 U 87 U 100 U 100 U GAMMA-CHLORDANE 89 u 100 U 89 U 8 7 U 100 U 100 U I TO!APHENE 180 u 200 U 180 U 170 U 200 U 210 U AROCLOR-1016 89 u 100 U 89 U 87 U 100 U 100 U AROCLOR-1121 89 u 100 U 89 U 87 U 100 U 100 U ' AROCLOR-1231 89 U 100 U 89 U 87 U 100 U 100 U I AROCLOR-1242 89 u 100 U 89 U 87 U 100 U 100 U AROCLOR-1248 89 u 100 U 89 U 87 U 100 U 100 U AROCLOR·125l 180 u 200 U 180 U 170 U 200 U 210 U I AROCLOR-1250 180 u 200 U 180 U 170 U 100 U 210 U I PERCENT MOISTURE 10 20 10 8 20 23 I I I I 11 I
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VOl!.ATILE ORGANICS ANALYSIS DATA SHEET
I
f'.eyst,,ne DC• 06008 --04-,
_EPA SAMPLE NO.
C-30-WA
;_,3.t.:, n3m12: •:EYSTOl'JE '.::NV. •: ,:,nt r-a,.: t:
I Lab Code: KEYTX Case No.: 06008 SAS Ne,.: so,; No.: C30WA
Matr i '" (s,,i l /11 ater J l•ATEF:
Sample 1,,,;t/v,:,l: 5.0 (g/mL) t1b....__
Lab Sample ID: ·jl)061)1)8()3
Lab File ID: 5UOE..008Vc)3A
Level: (low1medJ LOW
% Moisture: not dee. I
Date F:e,: e i ved: f)E,/011·:11)
Date Analy=ed: l)f, / 1)5 / •~('
C,:, l Ltmn: (pack/cap) PACK Dilution ra,:t,)r: 1 . 0
C,\S NO. COMPOUND
CONCENTRATION UN ITS:
<ug/L or ug/Kg) UG/L
74-87-3-l--------Chl ,:,r omet hane
74-83-~-L-------Brom,~mett,ane ----------------:
I . -----------------75-01-4-r-------Vinyl Chloride _______________ .:
75-00-3-r-------Chloroethane ________________ _
75-09-~---------Methylene Chloride :
I -----------67-64-1---------Acetone : I ----------------------75-15-<J---------carbon Disulfide :
I -------------75-35-4---------1 1-0ichloroethene :
I ' -----------75-34-3---------1 1-Dichlor,,ethane :
I • -----------540-53-t)T-------1,:-oichl~r,,ett,ene (total) ___ :
67-66-3-r-------Chloroform __________________ _
107-06-2--------1 2-Dichloroethane : I . • -----------78-93-3---------2-Butanone : I -------------------11-55-6---------1 1 1-Trichlorcethane :
1 ' , --------
56-23-5-1-------Car bon Tetrachloride _________ :
108-05-41-------Vinyl Acetate ________________ :
75-27-4---------Br omodi chl or ,:,methane :
78-87-5-1-------1 2-Dichloropropane ---------:
I • ----------! 0061-0115------c i s-1, 3-0i ch l ,,ropropene ______ :
7'3-01-G---------Tr 1 ch 1,,r oethene
1?4-48-ll-------Dibromochloromei~i~;---------:
-·. I ~ . ---------, 7'3-00-5---------1 1 .a.-Tr 1 ,:hi oroethane ,
-I ' ' --------71--43-2-7-------Benzene _____________________ _
1 Ootil-0276------tr ans-I, 3-Di ,:t, I or ,,pr opene ___ _
75-25-2-1-------Bromoform ___________________ _
108-10-1-
1
-------4-Met hy l -2-F'ent anone ________ _
591-78-G-
1
-------2-He x an one __________________ _
1~7-18-4--------T !trachloroeth~ne -

I

------------
~9-~4-5---------1 1 2 2-Tetrachloroethane
I ..... I , , , ----108-88-3--------Ta l uene _____________________ _
I 08-·~o-7-L------,;t,i or,,ben: ene I ----------------100-41-4-r------Et hyl ben: ene ________________ _
1 t)0-42-5-r------St yr ene _____________________ _
1330-20-7!------Xylene (total) _______________ :
Q
!O :u
10 :ll
10 :u
10 :u
I I :0
I I :s
5 :u
5 :u
5 :u
~ :u _,
5 :u
5 :u
10 :u
~ :u _,
5 :u
10 :u
5 :u
5 :u
5 :u
5 :u
5 :u
5 :u
5 :u
5 :u
5 :u
10 :u
10 :u
5 :u
5 :u
5 :u
5 :u
5 :u
5 :u
5 :u
----------------------------------------------------------
FORM I VOA I /87 Re
000040
• I
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VOLATILE ORGANICS ANALYSIS DATA SHEET
Keystone DCI 06008 -<>4-E
_EPA SAMPLE NO.
C-SSA
L~b Name: KEYSTONE ENV. Contra~t: 17·3:80-04
Lab Code: f::EYT X Case N,o. : OE.008 SAS No.: SDG No. : C30WA
Matri:<: (sc,il/water) WATEP Lab Sample ID: 900600804
Sample wt/vol: 5. 0 (g/mL) ~ Lab File ID: 5U06008VO-I
Level: ( I ,:,w / med JL ==-0,.,_W __ Date Re,:eived: 06/01/'30
Z Moisture: n,:,t dee. Date Analyzed: OE./04/90
Column: (pack/cap) PACK Dilution Factor: ~1~-~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane _______________ _
74-83-9---------Bromomethane ________________ _
75-01-4---------Vinyl Chloride ______________ _
75-c)0-3---------Ch l •:1r oet han~-----------------
75-09-:::---------Met hy l ene Chi ,or i de __________ _
67-64-1----~----Acet,:,ne _____________________ _
75-15-0---------Carbon D1sulf1de ____________ _
75-35-4---------1, 1-Dichloroetflene __________ _
75-34-3---------1,1-Dichloroethane __________ _
540-59-1)--------t,2-0i 1:f1loroethene (total) __ _
67-66-3---------Chloroform __________________ _
107-06-2--------1,:-Dichloroethane __________ _
78-93-3---------~-Butanone __________________ _
71-55-6---------1,1, 1-Trichloroethane _______ _
56-23-5---------Carbon Tetrachloride ________ _
108-05-4--------Vinyl Acetate _______________ _
75-27-4---------Bromodichloromethane ________ _
78-87-5---------1,2-Dichloropropane _________ _
IOOE.1-0l-5------cis-1,3-0ichloropropene _____ _
79-01-6---------Trichloroethene ______________ :
124-48-1-------o·i br omoc h I or omet hane _________ :
79""'.0C)-S---------1,1,2-Trichloroethane _______ _
71~-2---------Benzene _____________________ _
100£.,1-02-6------trans-l, 3-Di chl oropropene ___ _
75-25-2---------Bromoform ___________________ _
108-10-1--------4-Methyl-2-Pentanone ________ _
591-78-6--------2-Hexanone __________________ _
127-18-4--------Tet r a,: h l ,,r oet hene ___________ _
79-34-5---------1,1,2,2-Tetrachloroethane ___ _
108-88-3--------T,, I uene _____________________ _
108-90-7--------Chlc,robenzene _______________ _
100-41-4--------Ethylbenzene ________________ _
100-42-5--------Styrene _____________________ _
1330-20-7-------Xylene (total) _______________ ,
' '
23
75
10
46
28
10
5
30
37
5
38
5
10
5
33
10
5
35
5
36
5
36 s
5
35
10
10 s
32
5
37 s s
5
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FORM I VOA 1/87
000049
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• IA Keystone DCe 06008 -<>4-E
VOLATILE ORGANI1:s ANALYSIS DATA SHEET _EPA SAMPLE im.
C-'30A L.>b Name: KEYSTONE ENV. Contract: 173280-04
Lab C,ode: f'.EYTX Case No.: 1)6008 SAS No.: SDG No.: C30WA
Matrix: Cs,)11/~ater) WATER Lab Samp I e ID: '3006008r-
Sample wt/vol: 5.0 (g/mL) t1b..._ Lab File ID: 6U060<)8'~"
Level: ( I ,,w/med) LOW Oat e Re,: ei ved: 06/07/90
X Moisture: not dee. Date Analyzed: 06/14/'30
Dilution Factor: £1L.◊~-­
CONCENTRATION UNITS:
(pack/cap) PAO'.
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chlorometf,ane ________________ :
74-83-9---------Bromomethane _________________ :
75-01-4---------Vinyl Chloride _______________ :
75-00-3---------1:h l ,:,r ,:,ethane _________________ :
75-03-2---------Methylene Chloride ___________ :
67-64-1---------Acetone ______________________ :
75-15-0---------Carbon Disulfide _____________ :
75-35-4---------1, 1-0ichloroethene ___________ !
75-34-3---------1, 1-Dichloroethane ___________ :
540-5·:f-O--------l, :.::-Di c hl,,:iroethene (t,::it al) ___ :
67-66-3---------c•iloroform ___________________ :
107-06-:--------1,:-0ichloroet•1dne ___________ :
78-93-3---------2-Butanone ___________________ !
71-55-6---------1. 1, I-Trichloroethane ________ :
56-23-5---------Carbon Tetrachloride _________ :
108-05-4--------Vinyl Acetate ________________ :
75-27-4---------Bromodichlorometfiane _________ :
78-87-5---------1,2-Dichloropropane __________ :
10061-01-S------cis-1,3-Dichloropropene ______ :
7'3-01-6---------Trichloroethene ______________ :
124-48-1--------Dibromochloromethane : 7g-oo-s---------1, 1,2-Trichloroethane ________ :
71""'43-2---------Benzene :
tl)061-02-6------trans-t,3-DichlQropropene ____ 1
75-25-2---------Bromoform ___________________ _
108-10-1--------4-Methyl-2-Pentanone ________ _
5'31-78-6--------2-Hexanone __________________ _
127-18-4--------Tetrachloroethene ___________ _
79-34-5---------1,1,~,2-Tetrachloroethane ___ _ 108-88-3--------Toluene _____________________ _
11)8-'30-7--------Chlorobenzene _______________ _
100-41-4--------Ethylbenzene _________________ ,
100-42-5--------Styrene ______________________ :
1330-20-7-------Xylene (total> _______________ :
• •
10
10
10
10
5
27
s s s s s
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10
s s
10
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s s s s
s s
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FORl'1 I VOA
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1/87
000083
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• IA Keystone DCI 06008 --04-
VOLATILE OR6MHCS 1\NALYS!S DATA SHEET _EPA SAMPLE NC
C-91A
Lab Name: KEYSTONE ENV. Contra,: t : 1 7'3280-t)4
Lab C,ode: f:!::YTX Case No.: 06008 SAS No.: SDG No.: C30WA
Matrix: (s,:-i l /wat~r) WATEP Lab S<imple ID: 900600825
Sample wt /vol: 5.0 (g/mL.l t!L_ Lab File ID: 4U060<)8V:5
Level: (I c,w/med) LOW Date Re,:ei ved: 06/07 /"30
1/. Moisture: not de-:. Date Analyzed: 06/15/'30
c.,1 umn: Cpa,:k/i:ap) PACK Dilution r act •Jr :
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) U<3/L
74-87-3---------Chloromethane _______________ _
7 4-83-9---------Br ,:,mome th an e ________________ _
75-01-4--------~Vinyl Chloride _______________ :
75-00-3---------Chloroethane _________________ :
75-09-2---------Methylene Chloride ___________ :
67-64-1---------Acetone ______________________ :
75-15-0---------Carbon D1sulf1de ____________ _
75-35-4---------1,1-Dichloroethene ___________ :
75-34-3---------1, 1-Di i: h l or ,,ethane __________ _
540-59-1)--------1,~-0ichloroethene (totdl) __ _
67-66-3---------Chloroform __________________ _
107-06-2--------1,2·-0i~>,loroethane __________ _
78-93-3---------:-Butanone __________________ _
71-55-6---------1,1, I-Trichloroethane _______ _
56-:3-5---------Carbon Tetrachloride ________ _
108-05-4--------Vinyl Acetate _______________ _
75-27-4---------Bromodichloromethane ________ _
78-87-5---------1,2-0ichloropropane _________ _
10061-01-5------cis-1,3-0ichloropropene _____ _
7'3-01-6---------Trichloroethene _____________ _
124-48-1--------0ibromochloromethane
79~-5---------1,1,2-Trichloroethane::::::::
71-;43-2---------Benzene _____________________ _
10061,-02-6------trans-l, 3-Di •:hi or,,propene ____ '
75-25-2---------Bromoform ___________________ _
108-10-1--------4-Hethyl-2-Pentanone ________ _
5'31-78-6--------2-Hexanone __________________ _
127-18-4--------Tet r ach l ,,r ,,et hene ___________ _
79-34-5---------1,1,2,2-Tetrachloroethane ___ _
1 <)8-88-3--------To I uene ______________________ ,
108-90-7--------Chlorobenzene ________________ :
100-41-4--------Ethylbenzene _________________ :
100-42-5--------Styrene ______________________ :
1330-20-7-------Xylene <total) _______________ :
24
38
10
36
7
16
5
31
37
5
41
5
10
5
32
10
5
37
5
37
5
45
5
5
42
10
10
5
42
5
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5
5
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FORM [ VOA
Cl
1/87
000090
R,
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• IA Keystone Dea 06008 --04-8
VOLATILE ORGANICS ANALYSIS DATA SHEET _EPA SAMPLE NO.
S-R!NSATE
Lab N~me: KEYSTnNE ENV. C:,:,n tr a,: t : 1 7'3:::'.30-04
Lab C,:,de: 1: EYT X Case No.: 1)61)08 SAS No.: ____ SDG No.: C30WA
Matrix: (:.,oil/water) WATER Lab Sa.np 1 e ID: ·300E.008 I 5
Sample wt/vol: 5.0 ( g / ml) t!.b...._ Lab Fi le ID: 5U06008VIS
Level: LOW Date Re,:eived: OE./02/90
X Moisture: not dee. Date Analy=ed: 06/04/90
Diluti,,n Fa,:t,,r: 1.0 (pa,: k /,: ap) F'ACK "-'--"----
CONCENTRATION UN ITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane _______________ _ 10 :u
74-83-9---------Bromomethane ________________ _ 10 : lJ.
75-01-4---------Vinyl Chloride _______________ : 10 :u
75-1)0-3---------Chloroethane _________________ : 10 :u
75-09-2---------Methylene Chloride ___________ : 8
57-64-1---------Acetone ______________________ : 10 :u
75-15-0---------Carbon Disulfide _____________ : s :u
75-35-4---------1, 1-Dichloroethene ___________ : 5 :u
75-34-3---------1, 1-Dichloroethane ___________ : 5 'U
540-53-0--------1,:-Di,:hloroett,ene (total) ___ : 5 u
67-66-3---------Chloroform __________________ _ ~ u ~
107-06-2--------1,:-Dict1loroethane ___________ : s u
78-93-3---------:-Butanone __________________ _ 10 u
71-55-6---------1, 1, 1-Trichloroethane _______ _ 5 u
56--.:3-5---------Carbi:in Tetrachloride ________ _ 5 u
108-05-4--------Vinyl Acetate _______________ _ 10 u
75--.:7-4---------Br omodi chl ,:,r omet hane ________ _ s u
78-87-S---------l,2-Dichloropropane _________ _ 5 u
10061-01-5------cis-1,3-Dichloropropene _____ _ 5 u
79-01-6---------Trichloroethene 5 'U
124-48-1------.:.-Dibromochloromethane ________ _ 5 u
79-1)9-5---------1, 1, 2-Tr i ,:h 1 oroethane _______ _
71~2---------Benzene
5 u
s u
lOOfJ-02-6------t rans-I, 3-Di ,:h 1 or,,propene ___ _ 5 u
75-iS-2---------Bromoform ___________________ _ s u
I 08-10-1--------4-Methy 1-2-Pen t an,,ne ________ _ 4 J
591-78-6--------2-He,anone __________________ _ 10 u
127-18-4--------Tetra.:hlorocthene ___________ _ s u
79-34-5---------1,1,2,:-Tetrachloroethane ____ : 3 J
I 08-88-3--------T,, I uene ______________________ : 5 u
108-90-7--------Chloroben:ene ________________ : 5 u
100-41-4--------Ethylbenzene _________________ :
100-42-5--------Styrene ______________________ :
1330-20-7-------Xylene <total) _______________ :
: ----------------------------------------------
5 u
s :u
5 :u
------------------
FORM I VOA 1/87 Re,
000126
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0
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...... ~-.....
IA
VOLATILE OR6ANICS ANALYSIS DATA SHEET
Keystone DCI 06008 --04-6
_EPA SAMPLE NO.
TRIPBLANK
Lab N,,me: KEYSTONE ENV. Contract: 17'3280-04
Lab C,:,de: K:EYTX Cc1se N,:,.: 06008 SAS No.: SDG No.: C30WA
Matri:,;: (s,:,i l /water) WATER Lab Sample ID: '300600821
Samp I e 1o1t /vol: 5.0 (g/mU t'.!b__ Lab Fi le ID: 4U06<)08V21
Level: ( lo1o1/med) LOW Date Received: 06/06/"30
I. Moisture: not dee. Date Analyzed: <)6 / 0'3 / '30
C,:,lumn: (pa,:k/,:ap) PACK DilutiQn ra,:tor: 1.0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L ,,r ug/Kg) UG/L
74-87-3---------Chloromethane _______________ _
74-93-3---------Bromomethane ________________ _
75-01-4---------Vinyl Chloride _______________ :
75-00-3---------Chloroeth~ne _________________ :
75-09-2---------Methylene Chloride ___________ :
67-64-1---------Acetone _____________________ _
75-15-0---------Carbon Disulfide ____________ _
75-35-4---------1,1-0ichloroethene __________ _
75-34-3---------1, 1-Dichloroethane __________ _
540-59-0--------1,2-Di~}1loroet}1ene (total) __ _
67-66-3---------Chloroform __________________ _
107-06-:--------1,2-Dic•11oroathano __________ _
78-93-3---------2-But anc,ne __________________ _
71-55-6---------1,1, I-Trichloroethane _______ _
56-23-5---------Carbon Tetrachloride ________ _
108-05-4--------Vinyl Acetate _______________ _
75-27-4---------Bromodichloromethane ________ _
78-87-5---------1, 2-Di •: h l ,,r op r opane _________ _
10061-01-5------r.is-1,3-Dichloropropene~-----
7'3-0 I -6---------Tr i ch 1 or ,,ethene _____________ _
124~48-1--------Dibromochloromethane ________ _
79~-~---------1,1,2-Trichloroethane _______ _
71-'43-2---------Benzene _____________________ _
10061-02-6------trans-1, 3-Di chi ,jr opropene ___ _
75-25-2---------Bromoform ___________________ _
108-10-1--------4-Methyl-2-Pentanone ________ _
591-78-6--------2-Hexanone __________________ _
127-13-4--------Tetr a,:h I or,jethene ____________ '
79-34-5---------1,1,2,2-Tetra~hloroethane ___ _
108-80-3--------Toluene _____________________ _
108-90-7--------Chlorobenzene _______________ _
I <)0-41-4--------Ethy I benzene ________________ _
100-42-5--------Styrene _____________________ _
1330-20-7-------Xylene (total) ______________ _
' '
10
10
10
10
5
21
5
5
5
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5
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FORM I VOA
Q
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1/87 Pe
000137
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VOLATILE 0Rt3AN I CS ANALYSIS DA TA SHEET
Keystone DCI 06008 --04-E
_EPA SAMPLE NO.
TRIPBLAM<
L3b Name: KEYSTONE ENV. C,,nt r a,: t: 1 7"3280-04 --------------·
Lab C,:,de: KEYTX Case No.: OE,1)()8 SAS No.: ____ SDG No,: C30WA
Matrix: rsoil/w4terl WATER Lab Samp 1 e ID: 9(H)600806
Sample wt/vol: 5,0 (g/mLJ t1b...._ Lab File ID: 5U06008V06A
Level: (!,:,w/medl LOW Date Received: 06/01/90
1/. Moisture: not dee. Date Analy=ed: 06/05/90
Column: (pa,: k /,: ap) PACfi Dilution Factor:
C:\S NO. COMPOUND
CONCENTRATION UN ITS:
(ug/L or ug/Kgl UG/L
74-87-3---------Chloromethane _______________ _
74-83-9---------Bromomethane ________________ _
75-01-4---------Vinyl Chl,:,ride ______________ _
75-00-3---------Chloroethane ________________ _
75-05-:---------Methylene Chloride __________ _
67-64-1---------Acetone _____________________ _
75-15-0---------Carbon Disulfide ____________ _
75-35-4---------1, 1-Dichloroethene __________ _
75-34-3---------1, 1-Dichloroethane __________ _
540-59-0--------1,~-Dichloroethene (total) __ _
67-66-3---------Chl,:,raform __________________ _
107-06-2--------1,2-0ichloroethane __________ _
78-93-3---------2-Butanone __________________ _
71-55-6---------1,1, 1-Trichloroethane _______ _
56-23-5---------Carbon Tetrachloride ________ _
108-05-4--------Vinyl Acetate _______________ _
75-:7-4---------Bromodichloromethane ________ _
78-87-5---------1, 2-Di chi ,~ropropano _________ _
10061-01-5------cis-1,3-Dichloropropene _____ _
79-01-6---------Trichloroethene ______________ l
124.::-48-1--------Di bromoc hl or amet hane _________ I
79~-5---------1, 1, 2-Tr i,:hl oroethane ________ I
71~43-2---------Benzene _____________________ _
!0061-02-6------t r an,;-1, 3-Di ,:hl -~ropropene ___ _
75-25-2--------Bromoform ___________________ _
108-10-1--------4-Methyl-:-Pentanone ________ _
591-78-6--------2-Hexanone __________________ _
127-18-4--------Tet Yachl or,:iethene ___________ _
79-34-5---------1,1,2,2-Tetrac~loroethane ____ ,
108-88-3--------Toluene ______________________ :
108-90-7--------Chlorobenzene ________________ :
100-41-4--------Ethylbenzene _________________ :
100-4~-5--------Styrene ______________________ :
1330-20-7-------Xylene (total) _______________ : . '
10
10
10
10
12
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5
5
5
s
5
10
5
5
10 s
5 s
5
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5
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·----------------------------------------------' -------------
FORM I VOA 1/87 Re·
000145
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• IA
VOLATILE ORGANICS ANALYSIS DATA SHEET
Keyst,,ne OCe 06008 -o4-E
EPA SAMPLE 110.
TRIPBLANt-
Lab Name: kEYSTONE ENV.
Lab C,ode: VEY TX Case N,:,. : 06008 SAS No.: ____ SDG No.: C30WA
Matri•: (3011/waterl WATER Lab Sample ID: 900600817
Sample wt/vol: 5.0 C:9/mU l'.!b._ Lab Fi le ID: 5U06008Vl7
Level: (l,,w/medl =L=D~W __ Date Re,:eived: 0E,/(>2/9(1
% Moisture: not dee. Date Analyzed: 06/05/90
C,:,l umn: (pa,:k/capJ PACK
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane _______________ _
74-83-9---------Bromomethane _________________ '
75-01-4---------Vinyl Chloride ______________ _
75-00-3---------Chloroethane ________________ _
75-09-2---------Methylene Chloride __________ _
E, 7-64-1---------A,: et one _____________________ _
75-15-0---------Carbon Disulfide ____________ _
75-35-4---------1, 1-Di~hloroethene __________ _
75-34-3---------1,t-Dichloroethane __________ _
540-59-0--------1,2-Dichloroethene ltotall __ _
67-66-3---------Chloroform __________________ _
107-06-2--------1,2-Di,:hloroQthane __________ _
78-93-3---------2-Butanone __________________ _
71-55-6---------1, I, 1-Trichlaroethane _______ _
56-23-5---------Carb,:in Tet r achl or i de ________ _
108-05-4--------Vinyl Acetate _______________ _
75-:7-4---------Bromodichloromethane ________ _
78-87-5---------1, 2-Di ch l ,,ropropane _________ _
!006!-01-5------cis-1,3-Dichloropropene _____ _
79-01-6---------Trichloroethene _____________ _
12~8-1--------Dibromochloromethane ________ _
79..00-5--------1, 1, 2-Tr i ~hi ,,roethane _______ _
71~~-2---------Ben:ene _____________________ _
10061-02-6------trans-l,3-Dichloropropene ___ _
75-25-2---------Bromoform ___________________ _
108-10-1--------4-Methyl-2-Pentanone ________ _
531-78-6--------2-Hexanone __________________ _
127-18-4--------Tetrachloraethene ___________ _
79-34-5---------1,1,2,2-Tetrachloroethane ___ _
108-88-3--------Toluene ______________________ :
108-90-7--------Ch!orobenzene ________________ :
100-41-4--------Ethylbenzene _________________ :
100-42-5--------Styrene ______________________ :
1330-20-7-------Xy!ene <total) _______________ :
• •
1.0
10 :u
10 :u
10 u
10 u
13 B
10 u
5 u
5 u
5 u
5 :u
5 :u
5 :u
10 :u
5 u
5 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
10 :u
5 :u
5 :u
5 :u
5 :u
5 :u
5 :u
5 :u
-----------------------------------------------------------
FORM I VOA
Q
l/87 Re·
000155
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• IA
VOLATILE ORGANICS ANALYSIS DATA SHEET
Keyston• DCI 06008 --04-8
_EPA SAMPLE NO.
X-RINSATE
Lab Name: KEYSTONE ENV. C,;nt r act: I 7"3280-04
Lab (:,:,de: t(EYTX Case N,:i.: 0£009 SAS No.: ____ SDG No.: C30WA
Matr1,: (soil/water) WATER Lab Sample ID: 9006008:0
Sample wt/v,ol: 5.0 (g/mL) t!!,__ Lab File ID: 4U06008V:Q
Level: llow/medl ~L~O~W __ Date Received: 06/06/90
% Moisture: not dee. Date Analyzed: 06/0g;90
Column: (pack/,:apl
CAS NO. COMF'OUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane ________________ :
74-83-9---------Bromomet•iane ________________ _
75-01-4---------Vinyl Chloride ______________ _
75-00-3---------Chloroethane ________________ _
75-09-:---------Metf,ylene Chloride __________ _
67-64-1---------A~etone _____________________ _
75-15-0---------Carbon Disulfide ____________ _
75-35-4---------1,1-Dichloroethene __________ _
75-34-3---------1,1-Dichloroetf,ane __________ _
540-59-0--------1,2-Dichloroetf,ene (total) __ _
67-66-3---------Chloroform __________________ _
107-06-2--------1,:-Di~hloroethane __________ _
78-93-3---------:-Butanone __________________ _
71-55-6---------1, I, I-Trichloroethane ________ ,
56-23-5---------Carbon Tetrachloride ________ _
108-05-4--------Vinyl Acetate _______________ _
75-27-4---------Br ,::imod i ch l oromet hane ________ _
78-87-5---------1, =-Di ch l or.:,pr,,pane _________ _
10061-01-5------cis-1,3-Dichloropropene _____ _
7g-01-6---------Trichloroethene ______________ ,
124-48-1--------Dibromochloromethane _________ :
7g-oo-5---------t, 1,2-Trichloroethane ________ :
71-43-2---~-----Benzene ______________________ :
1006·1-02-6------tr ans-I, 3-Di chi or,~propene ____ :
75-25-2---------Bromoform ____________________ /
108-10-1--------4-Methyl-2-Pentanone _________ :
591-78-6--------2-Hexanone __________________ _
127-18-4--------Tetra~hloroethene ___________ _
79-34-5---------1, 1, 2, 2-T et r a,: h l or oet hane ___ _
109-89-3--------Toluene _____________________ _
108-go-7--------Chloroben:ene _______________ _
100-41-4--------Ethylben:ene ________________ _
100-42-5--------Styrene _____________________ _
1330-20-7-------Xylene (total) ______________ _
1-0
10
10
10
4
8
5
5
5
5
5
5
10 s
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10
5
5
5
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FORM I VOA 1/87 Re·
000162
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• IA
VOLATILE OR(lAN I CS ANALYSIS DAT A SHEET
Keystone DCI 06008 -<>4-E
_EPA SAMPI..E NO.
X-RINSATE
Lab Na~e: KEYSTONE ENV. Contract: 179:80-04
Lab C,:,de: KEYTX Case N,:,.: 06008 SAS No.: ____ SOG No.: C30WA
Matri:.;: (s,:,il/1..1ater) WATEF' Lab S.amp I e ID: ':lOOE.00826
Sample wt /vol: ( g / ml) t:!b...._ Lab f'ile ID: 4U06008V:£.
Le•1e I : '1,:-iw/med) LOW Date Received: 06/07/90
% Moisture: not dee. Date Analyzed: 06/15/90
Column: (pa,:k/cap) PACK Ci lut i,:in F'a.ct,:ir: 1.0
CAS IJO. COMF'OUND
CONCENTRATION UN ITS:
(ug/L or ug/Kg) fJG/L
74-87-3---------Chloromethane _______________ _
74-83-9---------Br,Jmom~than~-----------------75-01-4---------Vinyl Chloride ______________ _
75-00-3---------Chloroethane ________________ _
75-09-:---------Methylene Chloride __________ _
67-64-1---------Acetone _____________________ _
75-15-0---------Carbon Disulfide ____________ _
75-35-4---------1,1-Dichloroet•,ene __________ _
75-34-3---------1,1-Dichloroethane __________ _
540-59-0--------1,2-Dichloroethene (total) __ _
67-66-3---------Chloroform __________________ _
107-06-2--------1,2-Dichloroethane __________ _
78-93-3---------:-Butanone __________________ _
71-55-6---------1,1, 1-Tric•,l~roethane _______ _
56-23-5---------Carbon Tetrachloride ________ _
I 08-05-4--------Vi ny I A,: et ate _______________ _
75-27-4---------Bromodichloromethane ________ _
78-87-5---------1,2-Dichloroprapane _________ _
10061-0l-5------cis-1,3-Dichloropropene _____ _
79-01-6---------Tr i ,: h I or -oet hene _____________ _
124~48-1--------Dibromochloramethane ________ _
79~-5---------1, I, 2-Tr i ,:hi oroethane _______ _
71-43-2--------Benzene ______________________ ,
10061-02-6------trans-1, 3-01 ,:h I aropropene ____ :
75-25-2---------Bromof or m ______________ . _____ :
108-10-1--------4-Methyl-2-Pentanone _________ :
591-78-6--------:-Hexanone ___________________ :
127-10-4--------Tetrac•,l•lr,,ett,eno ____________ :
79-34-5---------1,1,2,2-Tetrachloroethane ____ :
108-88-3--------Taluene ______________________ :
108-'30-7--------Chlaroben:ene ________________ :
100-41-4--------Ethylben:eno _________________ :
100-42-5--------Styrene ______________________ :
1330-20-7-------Xyleno <total> _______________ :
•
10
10
10
10
6
9
5
5
5
5
5
5
10
5
5
10
5
5
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----------------------------------------------' -------------
f'ORM I VOA
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1/87 Re•
000172
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• IA Kay5tone DCI 06008 -<>4-f
VOLATILE ORGANICS ANALYSIS DATA SHEET _EPA SAMPLE: NC.
X-RINSATE
Lc,b Name: l'.EYSTONE ENV. Contract: 179:3•)-c)4
Lab C,:,de: l<EYTX Case No.: 06008 SAS N,:,. : SDG No. : C30WA
M3trix: (soil/water) WATER Lab Sample ID: '300600816
Sample wt/vol: 5.0 (9/mU !:!!:._ Lab File ID: 5U06008V16
Level: ( 1 ow/med) LOW Date Re•: ei ved: 06/02/'30
% Moisture: not dee. Date Analyzed: 06/05/'30
(,:,1 umn: (pa,:k/cap) PACK Dilution Factor: 1.0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/K9J UG/L
74-87-3---------Chloromethane _______________ _
74-93-9---------Bromomethane ________________ _
75-01-4---------Vinyl Chloride _______________ :
75-00-3---------Chloroethane ________________ _
75-09-2---------Methylene Chloride ___________ ,
67-64-1---------Acetone _____________________ _
75-15-0---------Carbon Disulfide ____________ _
75-35-4---------1, 1-Dichloroethene __________ _
75-34-3---------1,1-Dichloroethane __________ _
540-59-0--------l,2-0ichloroet•,ene (total) __ _
6 7-66-3---------Ch l ,:ir ,:. form __________________ _
107-1)6-:--------1,2-0i~hloroethane __________ _
78-93-3---------~-Butanone __________________ _
71-55-6---------1,1, I-Trichloroethane _______ _
56-23-5---------Carbon Tetrachloride ________ _
108-05-4--------Vinyl Acetate _______________ _
75-:7-4---------Bromodi~hloromethane ________ _
78-87-5---------1,2-Dichloropropane _________ _
10061-01-5------cis-1,3-Dichloropropene _____ _
7'3-01-6---------Trichloroethene _____________ _
124-48-1-------Dibromochloromethane ________ _
7'3~-5---------1,1,2-Trichloroethane ________ ,
71 ~.3-2--------Ben z ene ______________________ :
10061-02-6------trans-l,3-Dichloropropene ___ _
75-25-2---------Bromoform ___________________ _
108-10-1--------4-Methyl-2-Pentanone ________ _
591-78-6--------2-Hexanone __________________ _
1 :7-18-4--------Tet r o,:h l ,:.r 1Jet hene ___________ _
7'3-34-5---------1,1,2,.2-Tetrachl-:iroethane ___ _ 108-88-3--------Toluene _____________________ _
108-90-7--------Chlorobenzene _______________ _
100-41-4--------EthylbenzenP. _________________ ,
100-42-5--------Styrene ______________________ :
1330-20-7-------Xylene (total) _______________ I
10
10
10
10
5
10
5
5
5
5
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5
10
5
5
10
5
5
5
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10
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5
5
-----------------------------------------------------------
FORM I VOA
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1/87 Re·
000182
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• lA Keystone DCI 06008 --E
VOLATILE ORGANICS ANALYSIS DATA SHEET _EPA SAMPLE NO.
KOPPERS
Lab Name: KEYSTONE ENV. Contra,: t: 1 7'3'280-!)4
Lab Cc,de: f,'.EYTX Case No.: 06008 SAS No. : SDG No.: C30WA
Matri:<: ( s,:,i l /water) SOIL Lab Sample ID: 900600830
Sample 1,1t/vol: 5.0 <glmU §__ Lab File ID: 4U06008V30
Level : ( l ,:,1,1/med) LOW Date Re,: ei ved: 0",/01/'30
'l. Moisture: not dee. _ll Date Analyzed: 06/12/'30
C,:,l umn: (pa,:k/,:ap) PACK Di luti,:,n Factor: 1.<)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane _______________ _
74-83-9---------Bromomethane ________________ _
75-01-4---------Vinyl c•,Ioride _______________ :
75-00-3---------Chloroethane ________________ _
75-O9-::---------Hethylene Chloride ___________ :
67-64-1---------Acetone ______________________ :
75-15-0---------Carbon Disulfide _____________ :
75-35-4---------1,1-Dichloroethene ___________ :
75-34-3---------1, 1-Di ch! or,Jethane ___________ :
540-59-0--------1,2-Dichloroetheno (total) ___ :
6 7-66-3-----·----Chl or,:. form ___________________ :
107-06-2--------t,2-0ichloroathane __________ _
78-93-3---------2-Butanone __________________ _
71-55-6---------1, 1, l -Tri ,:h l 1:iroethane _______ _
56-23-5--~------Carbon Tetrachloride ________ _
108-05-4--------Vinyl Acetate _______________ _
75-27-4---------Bromodir.hloromethane ________ _
78-87-5---------1,2-0ichloropropane _________ _
10061-<)l-5----i s-1, 3-0ichloropropene _____ _
7'3-01-6---------Trir.hloroethene _____________ _
124-48-1-------0ibromochloromethane _________ :
7'3-'00-5---------1 1 1,2-Trichloroethane ________ :
, 71-43-2---------Benzene ______________________ :
10061-02-6------tr ans-1, 3-Di chl ,,r,,propene ____ :
75~2~-2---------Bromoform ____________________ :
108-10-1--------4-Methyl-2-Pentanone _________ :
5'31-78-6--------2-Hexanone ___________________ :
127-18-4--------Tet ra,:h 1 or,:,etheno ____________ :
7'3-34-5---------1, t, 2, :::-Tetra.chi or,:ietha.ne ____ :
108-88-3--------Toluene ______________________ :
108-'30-7--------Chlorobenzene ________________ :
100-41-4--------Ethylbenzene _________________ :
100-42-5--------Styrene ______________________ :
133O-2O-7-------Xylene <total> _______________ :
12
12
12
12
13
18
10
6
6
6
6
6
12
6
6
12
6
6
6
6
6
6
6
6
6
12
12
6
6
6
6
6
6
6 : -----------------------------------------------------------
FORM I VOA
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:u :u :u :u :u
·u u u u u u u u u u
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1/87 Re•
000187
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VOLA Tl LE OR•3AN I CS ANALYSIS DA TA SHEET
Keystone ·oc1 06008 ---0-I-t
_EPA SAMPLE "°·
S-10-FB(O-.::)
LJb Name: KEYSTONE ENV. Contr~ct: 179:80 04
Lab C,:,de: ,:EYTX Case No.: OE.008 SAS N,,.: SDG No.: C30WA
Mutri:.:: (s,:.il/water) SOIL Lab Samp 1 e ID: 900600807
Sample wt/v,,l: 5. 0 (g/mU §__ Lab File ID: 4U06008V07
Level: (J ,,w/med J LOW Date Re,:ei ved: 06/02/90
:~ M,,i sture: not de•:. _M Date Analyzed: 06/08/90
Column: (pack/cap) PACI< Dilution F"actor: ~1~-~0 __ _
c.~s NO. COMPOUND
CONCENTRATION UNITS:
<ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane ________________ : 15
74-83-~---------Bromomethane _________________ : 15
75-01-4---------Vinyl Chloride _______________ : 15
75-c)fJ-3---------Ch 1 oroethane _________________ : 15
75-09-2---------Methylene Chloride ___________ : 43
E, 7-EA-1---------A,: et ,,ne ______________________ : 160
75-15-0---------Carbon Disulfide _____________ : 8
75-35-4---------1,1-0ichl,~roethene ___________ : 8
75-34-3---------1,1-Dichloroethane ___________ : 8
540-59-0--------1,:-0ichlcroett,ene (total) ___ : 8
E, 7-66-3--------·-Chl or,:, form ___________________ : 8
107-06-:--------1,2-0ic>,loroethane ___________ : 8
78-93-3---------2-Butanone ___________________ : 15
71-55-6---------1, 1, 1-Tr i ch l •:ir,:iethane ________ : 8
56-23-5---------Carbon Tetrachloride _________ : 8
108-05-4--------Vinyl Acetate ________________ : 15
75-:7-4---------Br omod i ch l or ,,methane _________ : 8
78-87-5---------1,2-Dichloropropane __________ : 8
10061-01-5------cis-l,3-Dichloropropene ______ : 8
79-01-6---------Trichloroethene ______________ : 8
124-48-1-----~--Dibromochloromethane _________ : 8
79-00-:5---------1,1,2-Trio:hloroethane _______ _ 8
71-43-2---------Benzene _____________________ _ 8
10061-02-6------t rans-I, 3-Di ,:h 1,,r,,propene ___ _ 8
7:5-25-2---------Bromoform ___________________ _ 8
108-10-1--------4-Methyl -2-Pentan,,ne ________ _ IS
59 t -78-6--------2-He :-.· an,:,ne __________________ _ 15
127-\8-4--------Tetrachloroethene ___________ _ 8
7'3-34-5---------1, 1, 2, ::-Tet r a,:hl ,:,r ,~ethane ___ _ 8
108-88-3--------Toluene ______________________ : 8
108-90-7--------Chloroben=ene ________________ : 8
100-41-4--------Ethylbenz~ne _________________ : 8
100-42-5--------Styrene ______________________ : 8
1330-20-7-------Xylene <tot.all _______________ : 8 : ______________________________________________ : -------------
FORM I VOA
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B
B
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:u
:u
:u :u
:u :u :u :u :u
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1/87 Re
00019
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• IA Keystone DCI 06008 --v4-8
VOLATILE ORGANICS ANALYSIS DATA SHEET _EPA SAMPLE NO.
S-I 0-FB C:'.-4 J L.>b n,me: l(EYSTONE ENI/. C,:,n tr 3.•: t : 1 7'?"280-04
L.ab C,:,de: kEYTX Case 06008 SAS N,:,. : SDG No.: C30L.A
Matri~: (soil/water) SOIL Lab Sample ID: '300600810
Sample 1o1t/vol: 5.0 (g/mU §___ Lab File ID: 4U06008'J I 0
Level: ( 1 ,ow/med) LOI~ Oat e Re,: ei ved: 06/02/'30
X Moisture: not dee. Date Analy:ed: 06/08/'3<)
Column: (pack/cap) PACK Di l u t i ,:,n F" act or : 1 . O ~~--
CONCENTRATION UN I TS:
COMPOUND (ug/L e>r ug/l<g) UG/V.G a
74-87-3---------Chloromethane _______________ _ 13 : ti
74-83-9---------Bromomethane ________________ _ 13 :u-
75-01-4---------Vinyl Chle>ride ______________ _ 13 at
75-00-3---------Cfiloro~thane ________________ _ 13 :U
75-0'3-2---------Methylene Chloride __________ _ 16 :8 67-64-1---------Acetone _____________________ _ 160 :s
75-15-0---------Carbon Disulfide ____________ _ 6 :u
75-35-4---------1,1-Dichle>re>ethene __________ _ 6 :u
75-34-3---------1, 1-Di ,:hl ,:,r oethane ___________ , 6 :u
540-59-0--------1,2-Di~hloroethene <total> ___ : 6 :u
67-66-3---------Chloroform __________________ _ 6 :u
107-06-~--------l,2-Dichloroethane ___________ : 6 u
78-93-3---------:-Butanone __________________ _ 13 u
71-55-6---------1,1,1-Trichloroethane ________ : 6 u
56-23-5---------Carbon Tetrachloride ________ _ 6 u 108-05-4--------Vinyl Acetate _______________ _ 13 u
75-:7-4---------Bromodichloromethane ________ _ 6 u
78-87-5---------1,2-Dichlore>propane _________ _ 6 u
10061-01-5------cis-l,3-0ichloropropene _____ _ 6 u 7'3-01-6---------Trichloroethene _____________ _ 6 u
124-48-1--------0ibromochloromethane ________ _ 6 u
79-00-5---------1, 11 2-Tr i chi or,oethane _______ _ 6 u 71-43-2---------Benzene _____________________ _ 6 :u
1006i-02-6------trans-1,3-Dichlore>propene ___ _ 6 :u
75-25-2---------Bromoform ___________________ _ 6 :u
108-10-1--------4-Methyl-2-Pentanone ________ _ 13 u
591-78-6--------2-Hexanone __________________ _ 13 u
1:7-18-4--------Tetrach J ,,rc,ethene ____________ • 6 u
79-34-S---------l,I,2,2-Tetrachloroethane ___ ~ 6 u 108-88-3--------Toluene _____________________ _ 6 u
108-'30-7--------Chlorobenzene _______________ _ 6 u
100-41-4--------Ethylbenzcne ________________ _ 6 u 100-42-5--------Styrene _____________________ _ 6 u
1330-20-7-------Xylene Cte>tal> _____________ _ 6 u
' '----------------------------------------------------------------
FORM I VOA 1/87 Rev
000210
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• IA Keystone DCI 06008 --04-I
VOLATILE OP1:;ANICS ANALYSIS DATA SHEET _EPA SAMPLE NO
S-IO-FBC2-4D
LJb Nam■: kEYSTONE ENV. (ontract: 1·19:ao-1)4
Case No.: 06008
Matri:,;: < s,:ii 1 /1..iater) SOIL
Sample 1.Jt/vol: 5.0 ig/mL)
Level: (low/ med) LOW
M,:.i sture: no:it dee. ~~ ,. ~
Column: ( p,3,: k/,: ap) PAO'.
CAS NO. COMPOUND
§__
SAS No.: SDG No.: C30WA
Lab Sample ID:
Lab File ID:
Date Rei:ei ved;
Date Analyaed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L ,,r ug/Kg) U•3/KG
900600811
4U06008V11
06/02/90
06/08/90
1.0
Q
74-87-3---------Chloromett,ane ________________ l 13 : tt
74-83-9---------Bromomethane ________________ _ 13 :u :~
75-01-4---------Vinyl Chloride _______________ :
75-00-3---------Chloroethane _________________ :
13 ;~ 13
75-09-:---------Methylene Ct1loride ___________ : 14 :B
67-64-1---------Acetone _____________________ _ 120 1B
75-15-0---------Carbon D1sulf1de ____________ _ 6 :u
75-35-4---------1, 1-Di~hloroethene __________ _ 6 :u
75-34-3---------1, 1-Dichlorcethane __________ _ 6 :u
5-i0-59-0--------1,:-Di~hloroethene (total) __ _ 6 :u
67-66-3---------Chloroform __________________ _ 6 :u
107-06-2--------1, 2-D i ,: h 1 ,:,.y ,,ethane __________ _ 6 'U
78-93-3---------2-Butanone __________________ _ 13 u
71-55-6---------1,1, I-Trichloroethane _______ _ 6 u
56-23-5---------Carbon Tetrachloride ________ _ 6 u 108-05-4--------Vinyl Acetate _______________ _ 13 u
75-=-7-4---------Br omod i ch 1 or ,::imet hane ________ _ 6 u
78-87-5---------1, 2-Di ch l ,,ropr,::ipane __________ : 6 u
10061-01-5------cis-1,3-Dichloropropene ______ : 6 'U
7~-01-6---------Trichloroethene ______________ : 6 u
124-48-1--------Dibromochloromethane _________ : 6 u
79-:(?0-5---------1,1,2-Trichloroethane ________ :
71-43-2---------Benzene :
6 u
6 u
100&1-02-6------trans-1,3-Dichloropropene ____ : 6 u
75-25-2---------Bromoform ____________________ : 6 u
108-10-1--------4-Methyl-2-Pentanone _________ : 13 u
591-78-6--------2-Hexanone ___________________ : 13 u
127-18-4--------Tet ra,:h 1,,roethene ____________ : 6 ,U
79-34-5---------1,1,2,~-TetracJ,loroethane ____ : 6 :u
108-88-3--------Toluene ______________________ : 6 :u
108-90-7--------Chlorobenaene ________________ : 6 :u
100-41-4--------Ethylbenzene _________________ : 6 :u
100-42-5--------Styrene ______________________ : 6 :u
1330-20-7-------Xylene (total) _______________ : 6 :u
' ' ·----------------------------------------------' -----------------
FORM I VOA 1/87 Re·
000220
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IA Keystone oc• 06008 ~-e
VOLATILE ORGANICS ANALYSIS DATA SHEET _EPA SAMPLE NO.
S-13A-FB<0-2
Lab Name: KEYSTONE ENV.
Lab C,ode: KEYTX Case Ne-.: 06CH)8 SAS N,,.: ____ SDG No.: C30WA
Mat.r i :(: (s,:,i l /water) SOIL Lab Sample ID: 900600812
Sample ,.,t/v,:,l: 5.0 (g/mL) §___ Lab File IO: 4U06008Vl2
Level: ( I c,w/med l LOW Date Received: ()F,/02/90
% Moisture: not dee. Date Analyzed: 06/08/90
(,:, 1 umn: Cpad/cap) PAO'. Dilution Factor: &1&-~0~--
CONCENTRATION UNITS:
CAS NO. COMPOUND <u9/L or ug/Kgl UG/KG Q
74-87-3---------Chloromethane _______________ _ 13 : ~-
74-8:-3---------Bromomethane ________________ _ 13 :~
75-01-4---------Vinyl Chloride ______________ _ 13 : 1.1
75-0(1-3---------Ch 1 or oet hone ________________ _ 13 :u
75-o·:1-:---------Met hy 1 ene Ch 1 or i de __________ _ 16 :e
67-64-1---------Acetone _____________________ _ 82 :e
75-15-0---------Carbon Disulfide ____________ _ 6 :u
75-35-4---------1,1-Dichloroethene __________ _ 6 :u
75-34-3---------1, 1-Dichloroethane __________ _ 6 :u
540-S.'3-0--------1, 2-Di ,: h 11:-r .;iet. hene ( ti:it al ) __ _ 6 :u
67-66-3---------Chloroform ___________________ : 6 :u
107-1)6-2--------1,2-Dichloroethane ___________ : 6 :u
78-93-3---------2-Butanone ___________________ : 13 :u
71-55-6---------1,1,1-Trichlaraethane ________ : 6 :u
56-.:3-5---------Car bon Tet r achl ,:ir 1 de ________ _ 6 :u
108-05-4--------Vinyl Acetate ________________ : 13 :u
75-27-4---------Bromodichloromethane _________ : 6 :u
78-87-5---------1,2-Dichlaroprapane __________ : 6 :u
10061-01-5------cis-1,3-0ichloropropene ______ : 6 :u
79-01-6---------Trichloroethene ______________ : 6 'U
124-48-1--------0ibromochloromethane ' 6 u
79~.-5--------1, I, 2-Tr i ,:hi oroethane _______ _
71~3-c2--------Benzene _____________________ _
10061-02-6------trans-1, 3-0i chi ,,rapr,:,pene ___ _
6 u
6 u
6 u
75-25-2---------Bromoform ___________________ _ 6 u
108-10-1--------4-Methyl-2-Pentanane ________ _ 13 u
591-78-6--------2-Hexanone ___________________ . 13 u
127-18-4--------Tet r a,: h l ,:,r oethene ___________ _ 6 u
7·3-34-S---------1, 1, 2, 2-Tet r a,:hl oroethane ___ _ 6 u
108-88-3--------Toluene _____________________ _ 6 u
108-90-7--------Chlorabenzene _______________ _ 6 u
100-41-4--------Ethylbenzene ________________ _ 6 u
100-42-5--------Styrene _____________________ _ 6 u
1330-20-7----.---Xyl ene (total) ______________ _ 6 u
----------------------------------------------------------------
FORM I VOA 1/87 Rev
000230
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• IA Keystone DCa 06008 --04-G
VOLATILE ORGANICS ANALYSIS DATA SHEET _EPA SAMPLE NO.
S-13A-FB(>4
Lab Name: KEYSTONE ENV.
Lab Code: KEYTX Case No.: 06008 SAS No.: SDG No.: C30WA
Matri•: (soil/water) SOIL L3b Sample ID: 900600813
Sample wt/v,~l: s.o (g/mU §__ Lab File ID: 4U06008Vl3
Level: LOW Date Received: 06/02/91)
% Moisture: not de~. 22 Date Analy=ed: 06/08/90
C,:il umn: (pack/cap) PACK Dilution Fa,:t,:ir: 1.0
CAS NO. COMPOUND
CONCENTRATION UN ITS:
(ug/L or ug/Kgl UG/KG
74-87-3---------Chloromethane _______________ _
74-83-9-------·--Bromomethane ________________ _
75-01-4---------Vinyl Chloride _______________ ,
75-00-3---------Chloroethane ________________ _
75-03-2---------Methylene Chloride __________ _
67-64-1---------A~etone _____________________ _
75-15-0---------Carbon Disulfide ____________ _
75-35-4---------1,1-Dichloraethene __________ _
75-34-3---------1,1-Dichloroethane __________ _
540-59-0--------1,2-0i~>,loroethene (total) __ _ 67-66-3---------Chloroform __________________ _
107-06-~--------1,:-0i~hloroothane __________ _
78-93-3---------:-Butanone __________________ _
71-55-6---------1, 1, l-Tri1:hloroethane _______ _
56-:3-5---------Carbon Tetrachloride ________ _
108-05-4--------Vinyl Acetate _______________ _
75-27-4---------Bromc,d 1 ch 1 or omet hane ________ _
78-87-5---------1, 2-Di ch l ,,r opr ,:,pane _________ _
10061-01-5------cis-1,3-Dichloropropene _____ _
79-01-6---------Trichloroethene _____________ _
124-48-1---~----Dibromochloromethane
79~-~----~----1,1,2-Trichloroethan;::::::::
~~A!~:~;=~======:~~~:~~;3:oichi~;~P;~p;~;:::: 75~5-2---------Bromoform ___________________ _
108-10-1--------4-Methyl-2-Pentanone ________ _
591-78-6--------2-Hexanone __________________ _
1'27-18-4--------Tetrachloroethene ___________ _
7"3-34-5---------1, I,::, 2-Tet r a,:hl •~•oethane ___ _ 108-88-3--------Toluene _____________________ _
I 08-30-7--------Ch I or,,benz ene _______________ _
100-41-4--------Ethylben.:ene ________________ _
100-42-5--------Styrene _____________________ _
1330-20-7-------Xylene (total) ______________ _
13
13
13
13
21
47
6
6
6
6
6
6
13
6
6
13
6
6
6
6
6
6
6
6
6
13
13
6
6
6
6
6
6
6
-------------
FORM I VOA
Q
u
ti
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ti
B
B u
,U
u u u u u
u u u u u u u u u :u :u :u :u :u :u :u :u :u :u :u :u
1/87 Re·
000239
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IA Keyst,:,ne DCI 06008 --o4-!
VOLATILE ORGANICS ANALYSIS DATA SHEET _EPA SAMPU; NO.
X-1-0SN<0-2)
L..Jb N.>mo: KEYSTONE E~l'J. Contract: 179280-04
Lab C,:,de: KEYT X Case Nc1. : 06008 SAS No.: SDG No.: C30WA
Matri:(: (s,:,i 1 /1..1ater) SOIL Lab Sample ID: '3006008:::9
Sample wt /vol: _d.,..Q (g/mU G __ Lab File ID: 4U06008V:9
Level: (!ow/med) LOW Date Re,: ei ved: 06/07/'30
., Moisture: not dee. 20 Date Anal y:ed: 06/14/'30
C:,::il umn: (pack/,:ap) PACK Ci lutic,n F" a,: t,:ir: I. 0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L ,:,r ug/Kg) UG/KG Q
74-87-3---------Chloromethane _______________ _ 12 l/ ;
74-83-9---------Bromomet•ian~-----------------75-01-4---------Vinyl Chloride ______________ _
12 u
12 I)
75-00-3---------Chloroethane ________________ _ 12 u
75-0'3-2---------Methylene Chloride __________ _ 11 B 67-64-1---------Acetone _____________________ _ 15 B
75-15-0---------Carbon Disulfide ____________ _ 6 u
75-35-4---------1,1-0ichloroethene __________ _ 6 u
75-34-3---------1, 1-Dichloroethane __________ _ 6 u
540-59-0--------1,2-Dichloroethene (total) __ _ 6 u
67-66-3---------Chloroform __________________ _ 6 u
t07-06-:--------1,2-Dichloroet•1ane ___________ : 6 u
78-93-3---------2-Butanone __________________ _ 12 :u
71-55-6---------1, 1,1-Trichloroethane ________ : 6 :u
56-~3-5---------Carbon Tetrachloride ________ _ 6 :u
108-05-4--------Vinyl Acetate ________________ : 12 :u
75-27-4---------Bromodichloromethane ________ _ 6 :u
78-87-5---------1,2-Dichloropropane __________ : 6 :u
10061-01-5------cis-t,3-Dichloropropene ______ : 6 :u
7'3-01-6---------Trichloroethene ______________ : 6 :u
12~8-1-------Dibromochloromethane _________ :
79~-5---------1, I, 2-Tr i ,:hi or oethane ________ :
71-:-!'3-2---------Benzene ______________________ :
6 :u
6 :u
6 :u
10061-02-6------trans-1, 3-Di ch lor,:,propene ____ : 6 :u 75-25-2---------Bromoform ____________________ : 6 :u
108-10-1--------4-Methyl-2-Pentanone _________ : 12 :u
591-78-6--------2-Hexanone ___________________ : 12 :u
127-18-4--------Tetrachloroethene ____________ : 6 :u
7'3-34-5---------1,1,2,2-Tetrachloroethane ___ _ 6 u
108-88-3--------Toluene _____________________ _ 6 u
108-'30-7--------Chloroben:ene _______________ _ 6 u
100-41-4--------Ethylben:ene ________________ _ 6 u
100-42-5-----~--Styrene _____________________ _ 6 u
1330-20-7-------Xylene (total) ______________ _ 6 u
' '-----------------------------------------------------------
f"ORM I VOA 1/87 Re
000248
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VOLATILE OPGANICS ANALYSIS DATA SHEET
t<eystone DCI 06008 -<M-a
_EPA SAMPLE NO.
X-3'3-EA<O-:•
L3b N~mc: KEYSTONE ENV.
Lab Code: KEYTX Case No.: 06008 5;.5 Ne,. : 506 No.: C30WA
Matrix: (soil/water) SOIL Lab Samp I e ID: '300600814
Sample wt/vol: 5. 0 (g/mL) §__ Lab File ID: 4U06008V14
Level: <low/med) =L~O~W,__ Date Re,:eived: 06/02/'30
:~ Moisture: n,:,t de,:. 20 Date Analyzed: 06/08/'30
C.:il umn: (pa,:k/,:ap) PACK Dilution ractor: ~1~-~0 __ _
CAS NO.
CONCENTRATION UNITS:
(ug/L c,r ug/Kg) UG/KG
7 4-87-3---------Ch 1 or ,:imet h an e _______________ _
74-83-9---------Bromomethane ________________ _
75-01-4---------Vinyl Chloride _______________ :
75-00-3---------Chloroethane ________________ _
75-09-:---------Methylene Chloride ___________ :
6 7-64-1 ---------A,: et ,one _____________________ _
75-15-0---------Carbon Disulfide ____________ _
75-35-4---------1,1-Dichloroethene ___________ :
75-34-3---------1,1-Dichloroethane ___________ :
540-59-0--------1,2-Dic•lloroethene (total) __ _
67-66-3---------ct,loroform __________________ _
107-06-2--------1,2-0ichloroett,ane __________ _
78-93-3---------:-Butanone __________________ _
71-55-6---------1, I, I-Trichloroethane _______ _
56-23-5---------Carb•:>n Tet r ach l or i de ________ _
108-05-4--------Vi nyl A,: et ate _______________ _
75-27-4---------Bromodichloromethane ________ _
78-87-5---------1, 2-Di ,:h 1,,ropr,:,pane _________ _
10061-01-5------cis-1,3-Dichloropropene _____ _
7'3-01-6---------Trichloroethene _____________ _
124-:48-1--------Dibromochl,:,romethane
79~0-•------.:.--1 1 2-Tr i ,: h I oroethan;;;--------:
~-~ , , --------71:-43-2------.---Benzene :
101)6j-02-6--~---trans-1;3:otch10roprop;;;~;;;:::::
: . 7!5-25-2---------Br omo form ____________________ :
108-10-1--------4-Methyl-2-Pentan,:,ne _________ :
591-78-6--------~-Hexanone ___________________ :
127-18-4--------Tet r a,: h 1 or oet hene ___________ _
79-34-5---------1,1,~,2-Tetrachloroethane ____ :
108-88-:J--------T,) l uene ______________________ :
108-'30-7--------Chloroben:ene _______________ _
100-41-4--------Ethylbenzene _________________ :
100-42-5--------Styrene ______________________ :
1330-20-7-------Xylene Ctotal) _______________ :
12
12
12
12
16
10
6
6
6
6
6
6
12
6
6
12
6
6
6
6
6
6
6
6
6
12
12
6
6
6
6
6
6
6 ______________________________________________ I -------------
FORM I VOA
Q
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u u u
B
BJ u u u
,U :u :u :u :u :u :u :u
'U u u u u u u u
u u :u :u u
u
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u u
-----
1/87 Re
0002sc
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AWD Technologies, Inc.
APPENDIX A
RESULTS AS REPORTED BY THE LABORATORY
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IA Keystone DCI 06008 --04-,
VOLATILE ORGANICS ANALYSIS DATA SHEET _EPA SAMPLE NO.
X-46-WA
1_,b N.,me: KEYSTONE ENV. C,:,n tr a,: t : I 79280-04
Lab C,:,de: KEYTX Case No.: oe.ooe SAS No.: ____ SDG No.: C30WA
Matrix: (soil/water) SOIL Lab Sample ID: 900600819
Sample ,.,t /vol: 5.0 (g/mU §__ Lab rile ID: 4U06008V19A
Level: LOW Date Re,:ei ved: OE./06/90
Z Moisture: not dee. Date Analyzed: 06/11/90
C,:, l umn: (pa,: k /,: ap) P:\CK Dilution F"a,: tor: ~!~. ~C) __ _
CONCENTRATION UNITS:
CAS NO. COMF'OUND lug/Lor ug/Kgl UG/KG Q
74-87-3---------Chloromethane _______________ _
74-83-9---------Bromomethane ________________ _
12 :u
12 : t1 ' 75-01-4---------Vinyl Chloride ______________ _ 12 :u
75-00-3---------Chloroethane ________________ _ 12 :u
75-09-2---------Methylene Chloride __________ _ 70 :e
67-E.4-1---------Acetone _____________________ _ 12 :eJ
75-15-0---------Carbon Disulfide ____________ _ 6 :u
75-35-4---------l,1-Di..:hlorQethene __________ _ 6 :u
75-34-3---------1,1-Dichloroethane_~ _________ : 6 :u
540-59-C)--------l,2-Dichloroethene (total) ___ : 6 :u
67-66-3---------Chloroform __________________ _ 6 'U
11)7-06-2--------1,:-0ichloroethane ___________ : e. u 78-93-3---------:-Bu t an,:ine __________________ _ 12 u
71-55-6---------1,l, I-Trichloroethane ________ : 6 u
SE.-23-5---------Carbon Tetrachloride ________ _ 6 u
108-05-4--------Vinyl Acetate ________________ : 12 u
75-27-4---------Bromodichloromethane ________ _ 6 u
78-87-5---------1, 2-Di ,:h l oropr ,:,pane __________ : 6 u
10061-01-5------cis-l,3-Dichloropropene ______ : 6 u 79-01-6---------Trichloroethene ______________ : 6 u
124~A8-1--------Dibromochloromethane : 7~-,(jj)-5---------I 1 2-Trichloroethane ________ :
,. . -, , --------71-:i43-2--------Benz ene :
1oci4:t~2-6------trans-1;3:oi~h1o;op;ope~e====: 75-25~2---------Bromoform ____________________ :
6 u
6 u
6 u
6 u
6 ,U
108-10-1--------4-Methyl-2-Pentanono _________ : 12 :u
591-78-6--------2-Hexanone ___________________ : 12 :u
127-18-4--------Tetr cl•:hl ,:iri:iethene ____________ : 6 IU
79-34-5---------1, 1, 2, 2-Tet ra,:hl oroethane ____ : 6 :u
108-88-3--------T,,l ueno _____________________ _ 7
108-90-7--------Chlorobenzene _______________ _ 6 u 100-41-4--------EthylbP.nzenP. ________________ _ 6 u
100-42-5--------Styrene _____________________ _ 6 u
1330-20-7-------Xylene <total) ______________ _ 6 u : _____________________________________________ _ -------------
FORM I VOA 1/87 Rev
000268
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• IA Keystone DCI 06008 --0-1-c
VOLATILE ORGANICS ANALYSIS DATA SHEET _EPA SAMPLE NO.
X-7-LI'"
Lab Name: KEYSTONE ENV. C,,n tr .1,: t : I 7'3280-04
Lab C,ode: KEYTX 06008 SAS N,o, : ____ SDG No. : C30WA
Matr i" <.s-oi l /water) SOIL Lab Sample ID: '300600818
Samp I e wt /vol: 5.0 (g/mU _G __ Lab File ID: 4U06008V!BA
Level: <low/med) LOW Date Reo:eived: 06/06/'30
'l. Mc,i sture: not dee. ~ Date Analyzed: 06/11/'30
Di l u t i ,,n Fact or : ,.5c,,_,<)c_ __
CAS NO •. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) U13/KG
74-87-3---------Chloromethane _______________ _
74-83-9---------Bromomethane ________________ _
75-01-4---------Vinyl Chloride ______________ _
75-00-3---------Ch 1 ur ,:,ethane ________________ _
75-0'3-2---------Methylene Chloride __________ _
6 7-64-1---------A,: et ,:,ne _____________________ _
75-15-0---------Carbon Disulfide _____________ :
75-35-4---------1,1-Dichloroethene ___________ :
75-34-3---------1,1-Dichloroethane ___________ :
540-59-0--------1,2-Dichloroet•,ene (total) ___ :
67-66-3---------Chloroform __________________ _
107-06-:--------1,2-Dichloroethano __________ _
78-93-3---------2-Butanone __________________ _
71-55-6---------1,1,1-Trichloroethane _______ _
56-23-5---------Carbon Tetrachloride ________ _
108-05-4--------Vinyl Acetate _______________ _
75-27-4---------Bromodichloromethane ________ _
78-87-5---------1,2-Dichloropropane __________ :
10061-01-5------cis-1,3-Dichloropropene ______ :
7'3-01-6---------Trichloroethene ______________ :
124~48-1-------Dibromochloromethane :
7~-:S----· ----1, 1, 2-Tri ch l ,or oet hane:::::::: I
71~3-2------Ben.:ene ______________________ :
1006·1-02-6------tr ans-1, 3-Di chl or opropene ____ :
7:S~2:S-2---------Bromoform :
108-10-1--------4-Methyl-2-Peritanone _________ :
591-78-6--------2-Hexanone ___________________ :
127-18-4--------Tetrachlo>roethene ____________ :
79-34-5---------1,1,2,~-Tetrachloroethane ____ :
I 08-88-3--------ToJl •Jene ·---------------------:
108-'30-7--------Chloroben.:ene ________________ :
100-41-4--------Ethylbenzene _________________ :
100-42-5--------Styrene ______________________ :
1330-20-7-------Xylene (total) _______________ :
' •
65
65
65
65,
130
680
32
32
32
32
32
32
65
32
32
65
32
32
32
32
32
32
32
32
32
6:S
65
32
32
32
32
32
32
32
-----------------------------------------------------------
rORl'I I VOA
Q
u
u
11 u
B
B u u u u u u u u u
,U
:u :u :u :u :u :u :u :u :u :u :u •u u u u u u u
1/87
000283
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• 1A ~'.eyst on• DCI 06008 --04-E
VOLATILE ORGANI1:S ANALYSIS DATA SHEET _EPA SAMPLE NO.
X-'33
!_ab N.:imc: f(EYSTONE ENV. Contr.:ict: 179280-04
Lab C,:,de: KEYTX Case f'J-:,.: 0E.008 SDG No.: C30WA
Matrix: (soil/waterl SOIL Lab Sample ID: '3006008:?7
Sample wt/v,:,l: s.o (g/mL) §._ Lab File ID: 4U06008V:7
Level: (l.:,w/medl LOW Oate·Received: 06/07/9(1
'l. M,oi sture: not dee. _j_Q
Column: <pa,: k /,: ap l PACK
Date Analyzed: 06/14/'30
Dilution Factor: ,.1..,.,,oc__ __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/f(G
74-87-3---------Chloromethane ________________ :
74-83-3---------Br-,:imomethane ________________ _
75-01-4---------Vinyl Chloride _______________ :
75-00-3---------Chloroethane _________________ :
75-09-2---------Methylene Chloride __________ _
67-64-1---------Ac et ,:,ne _____________________ _
75-15-0---------Carbon Disulfide ____________ _
75-35-4---------1,1-Cichloroethene __________ _
75-34-3---------1, 1-Di chl Qr,jethane __________ _
540-59-0--------1,2-Dichloroethene (total) __ _ 67-66-3---------Chloroform __________________ _
tc)7-06-:--------1,:-0i,:hloroethane __________ _
78-93-3---------:-Butanone __________________ _
71-55-6---------1,1,1-Trichloroethane ________ ,
56-23-5---------Carbon Tetrachloride _________ :
108-05-4--------Vinyl Acetate ________________ :
75-27-4---------Bromodichloromethane ________ _
78-87-5---------1,2-Dichloropropane __________ l
!0061-01-S------cis-1,3-Dichloropropene ______ :
79-01-6---------Trichloroethene ______________ l
124-48-1--------Dibromochloromethane l
79j!O-:S---------l,1,2-Trichloroethane========
71.£C:3-2---------Benzene
10(!f,1-:-02-6------trans-1;5:01ch1~;~P;~pe~e::::
7:S~~-2---------Bromoform ___________________ _
108-10-1--------4-Methyl-2-Pentanone ________ _
591-78-6--------2-Hexanone __________________ _
127-!8-4--------Tetr.3chloroethene ___________ _
79-34-:S---------I, 1, 2, 2-Tetrachlorc,ethane ___ _ 108-88-3--------Toluene _____________ · _______ _
108-90-7--------Chlorobenzene _______________ _
100-41-4--------EthylbenzenP. ________________ _
100-42-:S--------Styrene _____________________ _
1330-20-7-------XylP.ne (total) ______________ _
11
II
11
11
'3
20
6
6
6
6
6
6
11
6
6
11
6
6
6
6
6
6
6
6
6
11
11
6
6
6
6
6
6
6
-----------------------------------------------------------
FORM I VOA
Q
:y
:u __;
:~ :u
:e :a :u :u :u :u :u :u :u :u :u :u :u :u :u :u :u :u :u :u :u :u :u :u :u :u :u :u :u :u
1/87 Re·
000293
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I E< f:.'eyst,:ine DC» (>E,1)1)9 -.)4-
SEMI VOLA Tl LE OF:13,;ri I ,:.S ,.\N,\L YS IS [',; T,; SHEET EF,.\ S,.\MFLc im.
LJb Na,ne: KEYSTONE ENV.
Lab C,:,de: 1:EYTX Case N,:,. : 05008 SAS N,:,.:
Matrix: (5,,il/water:, WATER Lab Sample IO: '3(l(JE,c)08"2':•
Samp 1 e •Nt I vo 1 : 1000 rg/mU t:1b.__ Lab File 10: -iuoe,o,,sc::::
(low/medl L~O~l~i __ Date Received: 06/07 /'30
% Moisture: not de,,:. de,:. Date Extra,: t ed: 06 / 0'3 I ·jl)
E:,.tra,:ti,:,n: CONT
1~PC Cleanup: pH: 7.0 Dilution factor: 1.0 ~-"----
'
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
11)8-35-~--------Pt,enol ______________________ _
111--l-l--l--------bis(2-ChlorcethyllEther ______ :
·;.S-57-8---------2-Ch l ,:,r ,:,phen,:,l _______________ :
541-73-1--------1,3-Dict,loroben:ene __________ :
106-46-7--------1,4-Dichlor,,benzene __________ :
100-51-E,--------8en:yl Alcohol _______________ :
35-50-1---------1,:-Di,,:t,l,,roben:ene __________ :
95--18-7---------2-Methylphenol _______________ :
3'?638-3-.::-·3------b is c.::-C:h l ,:,r ,:, i s,:,p r,:,p y 1 "i Et her __ :
1(:,6-44-5--------4-Mett,ylphenol _______________ :
621-64-7--------N-Nitroso-Di-n-Propylamine ___ :
67-7:-1---------He~achloroethane ____________ _
98-95-3---------Nitroben:ene ________________ _
78-59-1---------Isophorone ___________________ :
88-75-5---------2-Nitropt,enol ________________ :
105-67-9--------2,4-Dimethylpf,enol ___________ :
65-85-0---------Benzoic Acid ________________ _
lll-'31-1--------bis<:::-ChloroethoxylMethane ___ :
120-83-2--------2,4-0ichlorophenol ___________ :
120~02-1--------1,2,4-Trichloroben:ene _______ :
'31-20-3---------Naphthalene __________________ :
106-'47-8--------4-Chl or oani I 1 ne _____________ _
87-E,8-3---------Hexachlorobutadiene __________ :
59-50-7---------4-Chloro-3-Methylphenol ______ :
91-57-6---------2-Methylnaphthalene __________ :
77-47-4---------Hexachlorocyclopentadiene ____ :
88-1)6-2---------2,4,6-Tri~f,lor,,pf,enol ________ :
95-95-4---------2,4,5-Trichlorophenol ________ '
~1-58-7---------2-C>1lor,:,nap}1t>,alene _________ _
88-74-4---------:--Nitroaniline ______________ _
131-11-3--------0imethyl Phthalate __________ _
208-'36-B--------Acenaphthylene_~-------------
E,06-20-2--------2,6-Dinitrotoluen~ __________ _
Q
10 :u
10 :u
10 :u
10 :u
10 :u
I 0 :u
10 :u
1 (l :u
1 0 :u
10 :u
10 :u
10 :u
1 0 :u
10 :u
10 :u
10 :u
50 :u
10 :u
10 :u
10 :u
1 0 :u
10 :u
10 :u
10 :u
10 :u
10 :u
10 :u
50 :u
10 :u
50 :u
10 :u
10 :u
10 :u
'-----------------------------F □RM-I-SV-1 _____ _ ------------------1/87
000629
Re·
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1(
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _EF·A S,,MPL": NO.
Lab Name: kEYSTONE ENV.
Lab C,:,de: F'EYTX Case N,:,.: 05(,c)S SAS N,:,. :
M.itri~: 1.soil/water) WATER L..ib Sample ID: 'j(l1)f.,(H)8°2::.:
Sample wt/vol: 1 (ll)O (9/mU t!h._ Lab File ID: 4UOE.1)08C7.:
(!ow/med) ~LO~W~_ Date F:e,: ei ved: l)E,/1)7 /·31)
% Moisture: not dee. de,:. Date E, t r a,: t ed: OE./0·3/'30
E: ... tr a,: ti •:'In: ( SepF /C,:,n t /S,:,n,: )
GF'C Cleanup: (Y/N) tL_ pH:
,:·ONT
7. I)
Date Analy:Gd: OE,/~0/90
Dilution Factor: £1~-~0~--
CAS NO. C.OMF·OUND
CONCENTF:A TI ON UN I TS:
(ug/L or u9/K9) UG/L
·j9-09-:---------:-rA1troan1l1ne ______________ _
83-3:-9---------Acenapt,tt,ene _________________ :
51-28-5---------:,4-Dinitropt,enol ____________ :
100-02-7--------4-Nitr,~pf,enol ________________ :
13~-64-9--------Diben=,,furan ________________ _
121-14-:--------:,4-Dinitrotoluene ___________ :
84-E.E.-2---------Dietliylphthalate _____________ :
701)5-7~-3-------4-Cf1lorophenyl-pl1enylether ___ :
86-73-7---------Fluorene ____________________ _
100-10-6--------4-Nitr,,aniline ______________ _
534-52-1--------4,6-Dinitro-2-Methylp•ienol ___ :
86-30-6---------N-Nitrosodipl,enylamine Cll ___ :
l!)l-55-3--------4-Bromopt1enyl-pl1enylet•1er ____ :
118-74-1--------Hexachloroben:ene ___________ _
87-86-5---------Pentachl•Jropl,enol ____________ :
85-01-8---------Phenanthrene ________________ _
120-12-7--------Anthracene __________________ _
84-74-2---------Di-n-Butylphthalate __________ :
206~44-0--------rluoranthene ________________ _
12~;:00-0--------Pyrene _______________________ :
85-68-7---------Butylbencylphthalate _________ :
91-.94-1---------3, 3' -Di ch l ,:,r ,:,ben.: id i ne _______ :
56-55-3---------Benao(alAnthracene ___________ :
218-01-9--------Chrysene _____________________ :
117-81-7--------bis(2-Etliylhexyl1Phthalate ___ :
117-84-0--------Di-n-Octyl Phtha!ate _________ :
"20.5-·3•:f-2--------Benz,:., (b) r1 Lt•:,r .Jnthene ________ _
:07-08-9--------Benzo(~)Fluoranthene ________ _
50-32-8---------Benzo(a)Pyrene _______________ :
1~3-39-5--------Indeno(t,:,:-(d)Pyrene _______ :
53-70-3---------Dibenz(a,h)Anthracene ________ :
191-24-2--------Benzo(g,h,i)Perylene _________ :
50
10
51)
50
1 (l
10
ti)
I (I
10
5(l
51)
10
10
10
51)
10
10
10
10
10
10
20
10
10
3
10
10
10
10
10
10
10
-------------
Q
:u :u
:u :u
:u :u
:u :u
:u :u :u :u :u :u :u :u
:u
:u :u
:u :u :u
:u
:u
:J :u :u :u
:u :u
:u
:u
-----(!) -Cannot be separated from Diphenylamine
FORM I SV-2
000630
1/87 Re,
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• 18
SEMIVOLAT!LE ORGANICS ANAL\'SIS DATA SHEET EPA SAMF~S NO
Lab C,:,de: f EYTX SAS N,:,.: SDG N,:,.: C3(JW.:..
Matri·,.: 1s,:,il/•...,..3ter) l.JATEF' Lab Sample ID: '3(H)l:,(l(J8:::_·':
Sample 1,,,1t/v,:,l: 1000 (g/mL) !::!.b._ Lab Ftle ID: 4LJ06008C-~
Level: (low/med) L_o_w--Date F:e,: ei ved: <)E./07 /"30
% Moisture: not dee. de,:. Date Extracted: l)E, / (l'? / '?(l
E ... , tra•: ti ,:,r.: (SepF /C,:,nt /S,on,:)
(Y/N) I'.:!.__
Data Analy:ed: 051-.::01•:ii)
1~PC Cleanup: pH: Dilution ractor: =l=•-0 __ _
CAS NO. ,: 011F'OUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Pt,en,:,l ______________________ _
lll-44-4--------bis12-Chloroethyl)Ether ______ :
95-57-8---------2-Ct,l,:,r,:,pt,enol __ . ____________ :
541-73-l--------l,3-Dict1loroben:ene __________ :
106-46-7--------1,4-Dict,l,:,r,:,benzene __________ !
100-51-6--------Ben=yl Alcohol _______________ :
35-51)-1---------t,2-Di,:J,1,,r,:,ben:ene __________ :
35-48-7---------2-Met•iylphenal _______________ :
33638-3~-9------bis(:-CJ,l,)roisopr,,pyl )Ett,er __ :
!OE.-44-5--------4-Methylphenol _______________ :
621-64-7--------N-Nitr,~so-Di-n-Propylamine ___ :
67-7:-1---------Hexachloroethane ____________ _
38-9~-3---------Nitroben:ene ________________ _
78-59-1---------lsophorone ___________________ :
88-75-5---------2-NitropJ,enol ________________ :
105-67-9--------2,4-Dimethy!phenol ___________ :
65-85-0---------Benooic Acid ________________ _
111-91-1--------bisl:-ch!oroethoxylMethane ___ :
120-83-2--------2,4-Dichlorophenol ___________ :
120:92-1--------1, 2, 4-Tr i chl or,:iben:ene _______ :
91 ~20-3---------Napht h,; l enr, __________________ :
106.:.47-8--------4-Ch l ,oy,oan i 1 i ne _____________ _
87-68-3---------HexachloYobutadiene _________ _
59-50-7---------4-Chloro-3-Methylphenol ______ :
91-57-E.---------2-Methylnaphthalene __________ :
77-47-4---------He~ac•ilorocyclopentadiene ____ :
83-06-2---------2,4,6-Tri~hl 1)rophonol ________ :
95-95-4---------:,4,5-Tricfilorophenol ________ :
'31 -58-7---------~-Ch 1 or ,:,nap ht ha l ene __________ :
88-74-4---------2-Nitroaniltne ______________ _
131-11-3--------0imethyl Phtha!ate ___________ :
208-96-8--------Acenaphthylene _______________ :
606-20-2--------2,6-Dinitrotoluene ___________ :
Q
5E. :1
' :: 27
52
l<) :u
1 I) :u
10 :u
10 :u
10 :u
10 :.u
E.8
10 :u
14
10 :u
30
10 :u
10 :u
50 :u
10 :u
10 :u
10 :u
1 0 :u
10 :u
10 :u
10 :u
10 :u
10 :u
10 :u
5() :u
10 :u
50 :u
~ :J ~
10 :u
10 :u
----------------------------------------------------------------FORM I SV-1 1/87
000641
RE
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lC
SEMI '/OLA TI LE OF·,:;,,N I CS .\N,;L 'ISIS DATA s:,EET
keystone DCII 06008 -)4-
EF·A SAMF '....':: NO.
C-'31 A
Lab N.1me: kEYST□rJE ENV.
Lab (,:,de: t·EYT:i SDG N,:,. : C 30W:.
Lab S,3mple ID: ·3ooe.ooa::~
Samp I e 1,1t /v,:, I : 1000 Lab File ID: 4U06008C~
(!01,1/medl L~O~l~J __ Date Re,: ei ved: <)E.,,'1)7 /'30
½ Moisture: not dee. de,:. Date E.-,,:tra,: ted: 06 / 0·3 / "3<)
Extr,3.,: ti ,:,n: rsepF/Cont/Son,:) CONT Date Analyzed: 06/20/90
6F'C CleanLtp: (Y/N) N
,:,;S NO. COMPOUND
oH: 7.5
CONCENTRATION UN ITS:
(ug/L or u9/K9l UG/L
9'3-0~-2---------3-Nitro~nilina ______________ _
83-32-9---------A~enaohtt,ene ________________ _
51-~3-5---------:,4-Dinitr,)pt,en,)l ____________ :
101)-0:-7--------4-Nitropt,enol ________________ :
13:-64-9--------D1ben:,)f1Jr~n ________________ _
121-14-:--------:,4-Dinitrotoluene ___________ :
34-£6-:---------0iethylphthalate _____________ :
71)1)5-7:-3-------4-Chlor,~phenyl-pf,enylether ___ :
86-73-7---------Fluorene ____________________ _
100-10-6--------4-N1troan1l1ne ______________ _
534-5~-1--------4,6-Dinitro-2-Methylpt,enol ___ :
86-30-6---------N-Nitrosodipt,enylamine (1) ___ :
11)1-55-3--------4-Bromophenyl-phenyletf,er ____ !
118-74-1--------Hexachloroben:ene ___________ _
87-86-5---------Pentact1loropt1enol ____________ :
85-01-8---------Phenanthrene ________________ _
1~0-12-7--------Anthracene __________________ _
84-74-2---------Di-n-Butylphthalate __________ :
206-44-0--------Fluoranthene ________________ _
12~0-0--------Pyrene _______________________ '
85'-f,8-7---------Butylbenzylphthalate ________ _
'31-94-1---------3, 3' -Di ch 1 or ,::,ben: i dine ______ _
56-55-3---------Benzola)Anthracene __________ _
218-01-9--------Chrysene ____________________ _
!17-81-7--------bis(2-Ethylhexyl1Phthalate __ _
117-84-0--------Di-n-Octyl Phthalate ________ _
205-99-:--------Benzo(b)Fluorantt,ene ________ _
207-08-9--------Benzo(k)Fluoranthene ________ _
50-3:-8---------Benzo(a)Pyrene ______________ _
193-39-5--------Indenort,2,3-cd)Pyrene ______ _
53-70-3---------Dibenz(a,h)Anthracene _______ _
:1'31-24-2--------BenzoCg,h,i)Perylene _________ :
5t)
30
'3
50
1 <)
1 I)
10
10
10
50
50
10
11)
10
48
34
1 I)
10
10
30
10
20
10
1 <)
3
10
18
1 <)
1 0
I<)
I I)
19
-----------------------------------------------------------( 1 l -Cannot be separated from Di phenyl amine
Q
:u
:J :u
:u
:u :u
:u :u
:u
:u
:u
:u
:u
:J
:u :u :u
:u :u
:u :u
:J
:u
:u :u
:u :u
-----
~
FORM I SV-2 000642 1 /87 Re•
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IB
SEMIVOLATILE OPGANICS ANALYSIS DATA SHEET
Lab C,:,de: f'EYTX Case No.: !)60(18 SAS N,:,.:
L.ab Sample ID: 'j(l()E,1)1)8(1-:
Sample •~t/·1,:,l: 30.0 <g/ml) §__ Lab File ID: .JU060(i8C07
Level: ( l ,:,1,,,,1/m1:?d) LOW 03t2 Pc,: ei ved: 06/0:/·?(l
:~ M,:,isture: n,:,t de,:. 34 Date Extra,:ted: OE./06/·?0
E:,. tr-a,: ti ,:,n: c. SepF /C,:,n t /S,:,ni:) SONC
pH: 5.4 Di l Ll ti ,:,n Fact,::,,.-: 1 . l)O
CAS NO. 1:0MF'OUND
c·□NCENTRATI □rJ UNITS:
(L19/L ,:.r L19/K9.• UG/KG
l OS-'35-:.:------ --F'h en,:, l ______________________ _ 500
111-44-4--------bis(:-Chloroethyl)Ether ______ : 500
·35-57-8---------.::-Ch l ,:,r ,:,phen,.:il _______________ : 500
541-73-1--------1,3-Dichloroben:ene __________ : 500
1<)6-46-7--------1,4-Dichlorobenzene __________ : 500
100-51-6--------Ben:yl Alcohol _______________ : 500
·35-5()-1---------1,2-Dichloroben:ene __________ : .soo
~5-48-7---------2-Methylpf,enol _______________ : 500
39638-3:-9------bis(2-Ct,loroisoprc,pyl)Etf,er __ : 501)
106-44-5--------4-Methylp11en0l _______________ : 501)
6:1-64-7--------N-Nitr,J30-Di-n-Propylamine ___ : 500
67-72-1---------He~achloroethane ____________ _ 500 38-95-3---------Nitroben:ene ________________ _ 500 78-59-1---------Isophorone ___________________ : 500
88-75-5--·-------2-Ni tri::iphen,:,l ________________ : 500
105-67-9--------2,4-Dimethylpl,enol ___________ : 500 65-85-0---------Ben:oic Acid ________________ _ 2400
111-91-1--------bis(2-Chloroethoxy)Methane ___ : 500
1~0-83-2--------2,4-0ichloropt,enol ___________ : 500
120::82-1--------1, 2, 4-Tr i ,:h} ,:,r obenz ene _______ : 500 91-,20-3---------Naphthalene __________________ : 500
l06""47-8--------4-Chloroan1l1ne _____________ _ 500
87-68-3---------Hexachlorobutadlene __________ : 500
59-50-7---------4-Chloro-3-Methylphenol ______ ; 500 91-57-6---------=-Hcthylnaphtl,~lene __________ : 500
77-47-4---------Hexachlorocyclopentadiene ____ : 500
88-06-2-----~---2,4,6-Trichlor,,pheni::il ________ : 500
95-95-4---------2,4,5-Trichlorophenol ________ : 2400
il-59-7---------2-Chloronaphtf,alene __________ : 500
88-74-4---------2-N1troan1l1ne ______________ _ 2400
131-11-3--------Dimethyl Phthalate ___________ ; 5<)1)
208-96-8--------Acenaphthylene _______________ : 500
606-20-2--------2,6-Dinitrotoluene ___________ : 500
----------FORM I SV-1 -------------
0
' :u :u :u
:u :u
:u :u :u
:u
:u
:u :u
:u :u :u :u :u :u :u :u :u
:u :u :u :u :u :u :u :u
:u
:u :u :u
-----1/87
000729
Re,
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I ........ "'.
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1(
SEM l '/OLAT I LE OF·C,,\N l (3 ,\rJAL 'ISIS DAT A SHEET
f:eystone DC# <)E,008 -)-1-
EPA SAMPL:c NO.
S-lO-F81,:,-:)
L~b C,:,de: KEYTX (ase N,:,. : <)E,()08 SDG No.: C30WA
Lab s ... ,mp 1 e ID: 'jt)l)E,(H)SO 7
Sample t,,.1t /vol: 30.0 fg/ml) §__ Lab File ID: -4UOE.OOSC:1)7
(low/med)L =sO~W __ Date Re,:ei ved: l)E,/0:/'31)
Date E,;tra,:ted: OE,/ OE,/ ·?O
E:,. tr a,: ti ,:,n: ( SepF /C,:,nt I S,:,n,: J
(Y/NJ ~ pH:
D.at e Ana 1 yced: 06/ 1 ·:1 /':1(1
Di 1 u ti ,:,n Fa~ t ,:,r: I. 00
CAS NO. CCMF·OLJND
CONCENTPATION UNITS:
cug/L or ug/KgJ UG/KG
33-03-~---------3-~Jitroanilino _______________ : 2400
83-3:-9---------Acenapt,thene _________________ : 500
51-~8-5---------~,4-0initropf,en◊l ____________ : :-100
100-0:-7--------4-Nitrophenol ________________ : :400
132-64-9--------Diben:ofuran _________________ : 500
121-14-2--------2,4-Dinitrotoluene ___________ : 500
84-E,E,-:---------Diet.hylphth~late _____________ : 500
7005-7~-3-------4-Chlorophenyl-pf,enylether ___ : 5(11)
86-73-7---------rlu,,rene _____________________ : 500
100-10-6--------4-Nitroaniline _______________ : :400
534-5:-1--------,,,£-Dinitr,~-:-Met•iylptienol ___ : 2400
86-30-6---------N-Nitrosodipt,enylamine Cl) ___ : 500
101-55-3--------4-Br,,mophenyl-pt,enylett,er ____ : 500
118-74-1--------Hexachloroben=ene ___________ _ 500
87-86-5---------Penta~hloropt,enol ____________ : 241)1)
85-01-8---------Phenantt,rene ________________ _ 500
120-12-7--------Anthracene ___________________ : 5<)0
84-74-2---------Di-n-Butylphthalate __________ : 500
::::<)6-44-0--------Fl uor anthene : 50<)
129:.,00-0--------Pyrene _______________________ ; 500
85-68-7---------Butylbencylphthalate _________ : 500
91-94-1---------3, 3' -Di,: h l ,:,r ,:,benz i dine _______ : 1000
56-55-3---------Ben~o(a)Antt,racene ___________ : 500
218-01-9--------Chrysene _____________________ : 500
11 7-81 -7--------b is ( :-Et hyl11c,:yl j Phthal ate ___ : 100
117-84-0--------Di-n-Octyl Phthalate _________ : 500
205-99-2--------Ben=o(b)Fluor~nt•1ene _________ : ~00
:07-08-9--------Ben:o(kJFlu~rantl,ene _________ : 500
50-3:-a---------B~nzo(a)Pyrenc _______________ : 501)
133-33-5--------Indeno(t,2,3-cd)Pyrene _______ : 500
53-70-3---------Dibenz(a,t1)Antt1racene ________ : 51)1)
1~1-24-2--------BenzoCg,h,i)Perjlene _________ : 500
Q
:u
:LI :u
:u
:u
:u :u
:u :u :u :u :u :u
:u :u :u
:u :u :u
:u :u :u
:u :u
:J :u :u :u
:u
:u
:u :u
------------------
(I) -Cannot be separated from Diphenylamine
FORM I SV-2
000730
1/87 Re•
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I E<
SEM!VOLATILE CF:(iMJ!CS AN,',LYSIS DAT,> S1-'E:':T EPA SAMF~;: CIO.
L3b rJame: VEYSTONE ErlV.
Lab C,:,de: VEYTX SAS N,:,. : SDG N,:,. : (,3()W,:.
M.:\tri:-:: (•_;,:,il/•,,.1ater.1 SOIL L1b Sample I I:: ·j(H)6('1)81 •.:
Sample wt/v,:,J: 30.0 (g/ml) Id_ Lab File ID: 4U<}£008C: -:
Level: (low/med) ~L~O~W~-Date F:e,: ei ved: OE,/O::/·?o
% Moisture: not de~. de,:. Date E:~tra,:ted: 1)'=,/1)€,/'3('1
<'SepF /(,:,nt /S,:,n,:) Date Analysed: 0£/ ! '3/·3,:,
GF'C Cleanup: pH: 4.8 Cilution Factor: £1i-~O~O~--
CMS NO. ,:.OMF'OUND
1:m11:ENTF'ATIQr/ UNITS:
(ug/L or ug/t:g) UG/KG
1,)8-95-2--------Pt,en,~l ______________________ _ -V'1)
111-44-4--------bisi:-ChloroethylJEther ______ : 420
·35-57-8---------2-Chl•~rop ►,enol _______________ : 420
5·11-73-1--------1,3-Dichlorobenzene __________ : 420
106-46-7--------1,4-0i,:t1loroben:ene __________ : 420
100-51-6--------Ben=yl Alcot,ol _______________ : 420
35-50-1---------1,:-Dict,!,)roben:ene __________ : 420
·~5-48-7---------:-Mett,ylphenol _______________ : 42t)
33638-3:-·?------bi;<::-Ct,l,,r,,isopr,,pyl)Ett,er __ : 42()
106-44-5--------4-Methylphenol _______________ : -1::0
521-64-7--------N-Ni tr ,:is,:1-Di -n-Pr ,:,pyl amine ___ : 420
67-72-1---------Hexact,loroett,ane ____________ _ -1:0
98-95-3---------Nitrobenzene ________________ _ 420
78-59-1---------tsophorone ___________________ : 4:20
88-75-5---------2-Nitrophenol ________________ : 420
105-67-9--------2,4-0imett,ylpt,enol ___________ : 420
65-85-0---------Benzoic Acid ________________ _ 21 ()1)
111-91-1--------bis(~-Chloroetho•ylMethane ___ : 420
120~83-2--------2, 4-Di i:h l ,:ir ophen,:il ___________ :
12d;.e2-1--------l :: 4-Tr i ,:hl ,:ir,:,benzene : --, ' -------9 l:-'20-3---------Nap!,t ha! ene __________________ :
106~47-8--------4-Chloroaniline _____________ _
420
421)
420
420
87-68-3---------He•achlorobutadiene _________ _ 420
59-50-7---------4-Chloro-3-Methylphenol ______ : 420
91-57-6---------2-Mcthylnaphthalene __________ : 420
77-47-4---------Hexachlor,,cyclopentadiene ____ : 420
88-06-2---------~,4,6-Tri,:hlorophen,~1 ________ : 4:0
95-95-4---------2,4.5-Tri,hlorophenol ________ : 21 (H)
91-58-7---------2-Ct,1,,ronapt1thal2ne __________ : 420
88-74-4---------2-N1troan1!1ne ______________ _ 2100
131-11-3--------Dimethyl P•1tt1alate ___________ :
208-96-8--------Acenaphthylene _______________ :
420
420
606-20-2--------2,6-Dinitrotoluene ___________ : 420
Q
:u
:u :u
:u
:u :u
:u :u
:u
:u :u :u :u :u :u :u :u :u :u :u :u :u :u
:u :u :u
:u
:u :u
:u
:u :u :u
----------------------------------------------------------------FORM I SV-1 1/87 Re·
000758
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SEMII/OL,\TILE O!=·1:J1\NICS ,\fl,\L'.''31S Di'1T.~ SHEET
L .Jb n.11112: LEYS TONE El'J'.'.
Lab (,:,de: kEYTX Case I\J,:,.: (16()()8 SAS N,:,, :
~eystone DC# 06008 -04·
_EFA SAMF:..~ tJC
S-!<)-Fe1 :-4
S0t3 N,:i. : C3<)WA
Lab s.,mp I e ID: ·?,:101:.oos 1-J
Sample wt/vol: 30. c) (g/ml) ~ La1b File ID: 4UOE.OOBC:O
Levi:: l : (lDw/mcd) !=-=□~W~-D<ite Re,:ei ved: (>5/(J::/•:f('
X MoistL1re: not dee. de,:, Date E:,,tra,:ted: l)E,/(lE,/91)
{Sepr /C,:,nt /S,:,n,:)
GF'C Cleanup: (Y/Nl N pH: 4.8 Di 1 u t i ,:,n F ;1.,: t ,:,r : 1 • 00 ~~--
CAS NO. ,:□r1FOUND
CONCENTRATION UNITS:
(ug/L ,:,r Ltgn::g) U(:J/t-::G
33-0'3-:---------3-Nitr,~aniline ______________ _
83-3:-9---------A,:enaphthene _________________ :
51-28-5---------:,4-0initropt,enol ____________ :
:100
4:20
2100 1()0-02-7--------4-Nitrop•ienol ________________ :
13:-64-3--------Diben~ofuran ________________ _ ;: I 00
4:.20 121-14-:--------:,4-0initrotoluene ___________ : 420 84-&6-:---------Diethylphtl,alate _____________ ; 4:'.0
7005-72-3-------4-Ch l ,:,r ,:,phenyl-phenyl et her ___ : 4:0 86-73-7---------Flu,)renc ____________________ _ 4:20 100-10-6--------4-Nitroan1line ______________ _ .c I 00 534-5:-1--------4,6-Dinitro-:-Mett,ylpt,~nol ___ :
36-30-6---------N-Nitrosodiphenylamine (!) ___ :
101-55-3--------4-Bromopt,enyl-phenylether ____ :
118-74-1--------Hexachloroben:ene ___________ _
:: l (H)
4·.::o
42()
-i:o
87-86-5---------Pent ,lC h l ,::,r ,:,phen,:il ____________ :
85-01-8---------Phenanthrene ________________ _ 211)0
420 1~0-12-7--------Anthracene ___________________ :
84-74-2---------Di-n-Butylphthalate __________ : 420
➔::o 206-44-0--------Fluoranthene ________________ _ 4:'.0 1297-00-0--------Pyr'ene _______________________ :
85-68-7---------But yl b•?n: ,I phtha I ate _________ :
91-94-1---------3,3'-Dichloroben:idine _______ :
4::0
420
850 56-55-3---------Benzo(a)Anthracenc __________ _
218-01-9--------Chrysene _____________________ : 420
420
I I 7-8 I -7--------b i :a ( '.::-Et l1y I hex yl J Pht ha I ate ___ : 4'.20
117-84-0--------0i-n-Octyl Phthalate _________ ;
:05-39-2--------Benzo(b)Fluor~ntt,cne ________ _ 420
4~1)
:07-08-9--------Ben:ock,Fluorantfiene ________ _ 420
50-3~-8---------Ben:o(aJPyr~ne _______________ : 420
133-39-5--------Indeno(l,2,:-cd)Pyrene _______ : 4::0
53-70-3---------0ibenz(a,h)Ant•ira~ene ________ :
191-24-2--------Benzo(g,h,i)Perylene __ ~ ______ :
42t)
420
----------------------------------------------
Q
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(1) -Cannot be separated fr,,m Diphenylamine 000759
FORM I SV-2 I /87 Re•
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SEMIVOLATILE OPGANICS ANALYSIS DATA SHEET
S-12A-F:'· :-.::
Lab C,:,de: I EYTX s.;s N,:,. ,
Lab S.:imple ID: ';i:)(!t~(H)81 :_
30. 0 i'g/mL) §__ Lab File ID: -4U0513£C:::
(low/med) mL~O~W~_ D-3-1:e Pe,: e i ·1cid: ()l:,/0::1·;10
'l. Mcdsture: n,:,t dee. :.::3 de,:. Date Extra,:ted: 06 /OE./ ·30
(5,~pF /(:,:,nt /S,:,n,:)
(Y/N) ~ pH: 4.7 Dilution Factor: ~l~-~O~O~--
CAS NO. COMFOL.:NO
CONCENTRATION UNITS:
(ug/L c,r ug/tCg) UG/f~G
t08-~5-2--------Pt12nol ______________________ _ 430
111-44-4--------bisl.c-Chloroethyl )Ether ______ : 430
95-57-8---------:-Ct1lor,,pt1enol _______________ : 4.30
541-73-1--------1,3-Dichl,,roben:ene __________ : 430
1!)6-46-7--------1,4-0i,:t,lorob~n:ene __________ : 43(1
100-51-6--------Ben:yl Alcohol _______________ : 430
95-50-1---------1,2-Dict,lor,)ben:ene __________ : 430
95-48-7---------~-Methylpt,enol _______________ : 431)
33£38-3:-·3------bis(:-,:•,tor,:,isopr,:,pyl)Ether __ : 430
106-~4-5--------4-Mett,ylpt,enol _______________ : 430
£:1-64-7--------N-Nitr,~·;o-Di-n-Pr,,pylamine ___ : 430
67-7:-1---------He·.act,loroethane ____________ _ 430
38-95-3---------Nitroben:ene ________________ _ 430
78-59-1---------Is,Jpf,or(,ne ___________________ : 430
88-75-5---------2-Ni tr,:,pf)en,)l ________________ : 430
105-67-9--------2,4-Dimethylphenol ___________ : 430
65-85-0---------Benzoi~ Acid _________________ : 2100
111-91-1--------bisl2-Chloroethoxy)Methane ___ : 430
120~83-2--------2,4-Di~t1loropt1enol ___________ : 430
12'5::-82-1--------1, 2, 4-Tr i ,: h I ,:,r,:,ben::ene _______ : 430
91-20-3---------Nap•itt,~l~na __________________ : 430
10&.~'47-8--------4-Ch 1 ,::.roani 1 i ne ______________ : 430
87-68-3---------Hexact,lorobutadiene _________ _ 430
59-50-7---------4-Chloro-3-Methylphenol ______ : 43()
91-57-6---------2-Mett,ylnapt,t•i~lene __________ : 430
77-47-4---------Hexachlorocyclopentadiene ____ : 430
88-06-2----------:,4,6-Trichloropt1enol ________ : 430
95-95-4---------2,4,5-Tric•ilorophenol ________ : 2100
91-58-7---------2-Ct1loronJpht•1Jlene __________ : 430
88-74-4---------2-N1troan1!,ne ______________ _ 2100
131-11-3--------Dimethyl Phthalate ___________ : 430
208-96-8--------Acenaphthylene _______________ : 430
606-20-2--------2,6-Dinitrotoluene ___________ : 430
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' ' ' ·----------------------------------------------·-------------' FORM I SV-1
Q
1 /87 Re·
00080:J
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SEMI \/OLAT I LE or.·1jMN: ( S ,\M,;L YS IS 01\ TA SHEET
(!E.,c:,os
M.~ ~ r l :,: : ( 5,:, 1 l / i..;a t er ) SO! L L_,b Sdmple ID: '31)t)60<)8 l:
Samele wt/v,:,1: 30.() (g/mL) Ii.__ Lab File ID: 4UC)5136C::
llow/med) ~L~O~I~/ __ Date Pe,: ei ved: OE. I 1}::; ·30
:~ M,:li sture: n,:,t de,:. :::3 de,:. Date E:<tra,:ted: 0£./t)E,/·j(J
StJ!'-JC Date Analysed: (JE,/ l "3/'30
1.;):PC CI eanLtp: pH: 4.7 Di luti,:,n Fa,:t,:,r:
'
CAS NO. CCMF'CiUt!D
CONCENTF:I\ TI ON UN I TS:
!·ug/L or ug/Kg) UG/~G
:::100 83-3:-3---------Acenapfithene _________________ : 430 51-:::8-5---------:::,4-0initropJ,enol ____________ : 2100 100-():-7--------4-Nitr,~pf,enol ________________ : :2100 132-64-~--------0ibQn:ofuran _________________ : 431)
121-14-=--------2,4-Dinitrotoluene ___________ : 430
84-66-2---------Dicthylphthalate _____________ : 431)
7i)<)5-7:-3-------4-Chl,~ropt1enyl-pf1enylett1er ___ : 430 86-73-7---------Fluoreno ______________________ : 4.30
lQi)-10-6--------4-Nitroaniline _______________ : :100
534-5:-1--------4,6-Din1tro-:-Mett1ylpf1enol ___ : 2100
86-30-6---------N-Nitrosodiphenylamine (1) ___ : 430
101-55-3--------4-Brom,~pt1enyl-pf1cnylett1er ____ : 430
118-74-1--------Hexachloroben=ene ____________ : 430
87-86-5---------Pen~achl,Jropt,enol ____________ : :100 85-01-8---------Phenanthrene _________________ : 430
120-12-7--------Anthracene __________________ _ 430
84-74-2---------Di-n-Butylohthalate __________ : 430
206.'-'44-0--------n uor anthene _________________ : 430 12S-OO-O--------Pyrene _______________________ : 430
85-68-7---------Butylbenzylphthalate _________ : 430
91~~4-1---------3,3'-Dichlorobenzidine _______ : 860
56-55-3---------Ben:o(a)Antt,racene ___________ : 430
218-01-9--------Chrysene _____________________ : 430
117-81-7--------bis(2-Ethylhe,yl)Phthalate ___ : 430
117-84-0--------Di-n-Octyl F'hthalate _________ : 430
~05-99-2--------Ben=•)Cb:1Fl11oranthene __________ : 430
207-08-9--------Ben=oc•~)Fluoranthene _________ : 430
50-32-8---------Ben:o(a)Pyrene _______________ : 430
133-J3-5--------Indeno<t,:,3-cd)Pyrene _______ : 430
53-70-3---------Diben:Ca,t,)Antt,racene ________ : 430
191-24-2--------Benzo(g,h,i)Perylene _________ : 430
I. 00
0
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i1) -Cannot be separated from Diphenylamine ------------------
FORM I SV-2 000810 1/87 Re
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SEM!VOLATILE OPGANICS ANALYSIS DATA SHEET
s-iorsi:.-4.>D
Lab C,:,de: t•:EYTX Case N,:,. : OE.008 SAS N,:,. :
Matri·~: (soil/water) SOIL Lab Sample ID: '?0f)E,(H)8 ! :
Sample 1,1t/vc,l: 30.0 (g/ml) §__ Lab File ID: 4U06008C: !
Level: Date Pe,: ei ved: (16/(r.:,;·3,:,
½ Moisture: n,,t dee. de,:. Date Extra,:ted: 06/0E,/·:f(,
pH: ·l.b
Date Analy:ed: 06/:9/90
Dilution Factor: £1~-~0~0~--
,:As ,'JC. COMPOUND
,:IJNCENTF:A TI ON UN I TS:
1·ug/L or ug/Kg) UG/VG
11:•8-35-2--------P•ien,)l ______________________ _ 420
lll-44-4--------bisf2-Ch!oroethyl)Ether ______ : 420
~5-57-8---------:-1:hloropt,enol _______________ : 420
~41-73-1--------1,3-Dichloroben:ene __________ : 420
1,:16-46-7--------1, 4-Di ,: h l ,:ir,:,ben:: ene __________ : 4:::0
l0!)-51-6--------Ben:yl Alcot,ol _______________ : 420
~S-5c)-1---------1,:-Di~t1l,)r,)ben:ene __________ : 42(1
95-48-7---------:-Methylphenol _______________ : 4:0
3~638-3:-·~------bis(:2-C•iloroi~opr,:,pyl)Ether __ : 420
106-44-5--------4-Methylphenol _______________ : 4:20
621-64-7--------N-Nitroso-Di-n-Propylamine ___ : 4::'.I)
67-7~-l---------He~achloroetl,ane ____________ _ 4:21)
98-35-3---------Nitroben:ene ________________ _ 410
76-59-1---------Isophorone ___________________ : 421)
88-75-5---------2-Nitrophenol ________________ ! 4 :2()
105-67-9--------2,4-Dimethylphenol ___________ : 421)
55-85-0---------Benzoic Acid _________________ : 2100
111-91-1-------bi s <::-Chi or oet ho,y) Methane ___ : 420
120~63-2--------2,4-Dich!oropheno! ___________ : 420
12~82-1--------1, 2, 4-Tr i ch l or,:.ibenzene _______ : 420
31-~0-3---------N~phthalene __________________ : 4:':0
106-47-B--------4-Chloroan1!1ne _____________ _ 420
B7-6B-3---------Hexachlorobutadiene __________ : 421)
59-50-7---------4-Chloro-3-Methylphenol ______ : 420
91-57-6---------2-Methylnaphtha!ene __________ : 421)
77-47-4---------Hexachlorocyclopentadiene ____ : 420
88-<)6-:---------2,4,6-Trichlorophenol ________ : ~:::o
35-95-4---------2,4,5-Trichlorophenol ________ : 2100
31-58-7---------2-Chloronaphthalenc __________ : 4:<)
SB-74-4---------2-Nitroaniline _______________ : 2100
131-11-3--------Dimethyl Phtha!ate ___________ : 4~()
206-96-B--------Acenaphthylene _______________ : 420
606-20-2--------2,6-Dinitrotoluene ___________ : 420
Q
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----------------------------------------------------------------FORM I SV-1 1/B7
000781
Re·
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SEMIVOLATILE OPGANICS ANALYSIS DATA SHEET
Keystone DCM 05008 -)4-
_EPA SAMPLE rio.
S-IOFB<:--<,C
LBb N.ame: ~EYSTONE ENV.
Lab :.:,:,Ce: LEYTX SAS N,:,.: 5013 No.: C3(lWA
M~trix: (soil/water) SOIL L.1b Sample ID: "3005(>(>8 I I
Sample wt/v,:,l: :?0.0 (g/mL) §___ Lab File ID: 4U0500BC l:
Date Re,: ei ved: oe.10:1·10
% Moisture: not dee. __ de,:. Date E ., tr a,: t ed: 05/0E,/·,o
(SepF/Cont/Sonc) Date Analy:ed: <)5/ l'?/"3<)
pH: 4.5 Di 1 Ltt i ,:,n f" a,: tor:
(MS tJO. •:OMF'OUND
CONCENTRATION UNITS:
(L19/L or ug/t(gj UG/KG
93-03-:---------3-Nitr·,)aniline ______________ _ 2100 33-3:-~---------Acenaphtt,ene _________________ : 420
51-28-5---------2,4-Dinitr,)pt,~nol ____________ : :: 11)()
11)0-02-7--------4-Nitr,,ptienol ________________ : 2100
13~-64-'3--------Diben:ofuran ________________ _ 4·10
1:1-14-2--------2,4-Dinitr,)t,Jluene ___________ : 420
84-55-2---------Diethylphthalate _____________ : 421)
701)5-7:-:-------4-Ct1loropt1enyl-pt1enylett1er ___ : 4:0
86-72-7---------fluorene _____________________ _ 4:0:0
10,)-10-6--------4-Nitroaniline ______________ _ 2100
534-52-1--------4,6-Dinitro-:-Methylpt,cn,,l ___ : 2100
86-30-6---------N-Nitr•~sodiphenylamine (1) ___ : 420
101-55-3--------4-Bromophcnyl-phenylether ____ : 420
118-74-1--------Hexachloroben:ene ___________ _ 4:0
87-86-5---------Pentachlorop•ienol ____________ : 210<)
85-01-8---------Phenanthrene ________________ _ 420
120-12-7--------Anthracene __________________ _ 420
84-74-2---------Di-n-Butylphthalate __________ : 420
206-44-0--------Fluar~nthene ________________ _ 420
129:-()0-0--------Pyrene _______________________ : 420
85-68-7---------But yl ben: y I pht t,a 1 ate _________ : 420
91 -94-1---------3, 3' -Di,: h 1 ,:,r ,:,ben;: id i ne _______ : 850
56-55-3---------Benzo(alAntt,racene __________ _ 420
218-01-9--------Chrysene _____________________ : 420
117-81-7--------bisl2-Ethylhe,yllPhthalate ___ : 420
117-84-0--------Di-n-Octyl Phthalate _________ : 420
~OS-93-2--------Ben;:o<b1Fluoranthene ________ _ 420
207-08-9--------Benzorl lPlu,~rantt,ene ________ _ 420
50-3:-a---------Benzo(a)Pyrene _______________ : 420
193-39-5--------Indeno(l,2,3-cd)Pyrene _______ : 420
53-70-3---------Dibenz(a,h)Anthracene ________ : 4·20
191-~4-2--------Benzo(g,h,iJPerylene _________ : 420
1.00
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----------------------------------------------------------------(1) -Cannot be separated fr,,m Diphenylamine 000782
FORM I SV-2 I /87 Re,
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lB
SEMIVOLAT:LE ORGANICS ANALYSIS DATA SHEET EF'A SAMF'~~ ,"JO
Lab C,)de: f"EYTX (3se N,).: 1)6008 SAS N,:,.:
Lab S_;mp 1 e ! D: 'jf)()/:,(H)8 1,:
Samp I e 1,1t /v,:,l: 30.0 (g/ml) ~ Lab File ID: 4UOE,c)(JSC 1 ::!='
(1 ,:ii.J/med) LOW D.ate Pe,: ei ve,j: OE,/0:?/·jt)
de,:. Date E,. tr a,: ted: ()? 10::1·~0
E:,. t ra,: ti ,:,n: (ScpF/(,)nt/Sonc)
GF'C Cleanup: pH: 4.7 Dilution Factor: ~1~-~0~0~-
CA,' NO. ,:GMF'OUND
CONCENTF:AT I OIi uri I TS:
,·ug/L ,,rug/Kg) UG/KG
430
111-44-J--------bisf:-Cf1loroethylJEt!1er ______ : 430 35-57-8---------:-1:t1lor,,pt1enol ________________ : 430
541-73-1--------t,3-Dic!iloroben:ene __________ : 430
106-46-7--------1,4-Dic•il,)roben~ene __________ : 430 100-51-6--------Ben:yl Alcof1ol ________________ : 430
35-50-1---------1,:-0ict,lorc,ben:ene __________ : 430 95-48-7---------2-Mett1ylpt1enol _______________ : 430
39638-32-~------bis(:-Ct1l,)roisopropyl:1Ether __ : 430
106-~4-5--------4-Metfiylpt,enol _______________ : 430
6:1-64-7--------N-Nitroso-Oi-n-Propylamine ___ : 431)
£7-7:-1---------He•achloroethane ____________ _ 430
98-95-3---------Nitroben:ene ________________ _ 431)
78-59-1---------Isophorone ___________________ : 430 88-75-5---------2-Nitropt,enol ________________ : 430
105-67-9--------2,4-0imetf1ylpt1enol __________ :: 430 65-85-0---------Ben:01c Acid ________________ _ 2100
111-91-1--------bis(2-Chloroethoxy)Methane ___ : 430
1 :0-83-2--------2, 4-0i ,: h l or ,)phen,:,l ___________ : 430
120:82-1--------1, 2, 4-Tr i ch l or ,:-ben: ene _______ : 430
'31-:-;20-3---------Napht ha I ene __________________ : 430
106-47-8--------4-Chloroaniline ______________ : 430
87-68-3---------Hexact,lorobutadiene __________ : 430
5'3-50-7---------4-Ch l ,:,r,:,-3-Met hyl phenol ______ : 430
91-57-6---------2-Methylnaphthalene __________ : 430
77-47-4---------Hexachlorocyclopentadiene ____ : 430
88-06-~---------2,-i,6-Tri~f1loropt1cnol ________ : ·130
95-95-4---------:,..i,5-Trichloropt,enol ________ : 2100
'31-58-7---------2-(t, l ,:ir ,:,nap ht hal ene __________ : 430
88-74-4---------2-Nitroaniline _______________ : :::100
131-11-3--------Di methyl Pht h.> I ate ___________ : 430
208-'36-8--------Acenaphthylene _______________ : 430
606-20-2--------2,6-0initrotoluene ___________ ! 430
Q
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----------------------------------------------------------------FORM I SV-1 1/87 Re
000835
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_EPA SAMPL~ 110.
S-13.-\FB( <F:E
L"1b C,:,de: IEYTX Case N,:,.: 06(H)8
L~b S...1mp le !D: ·_;l()()E,,)()81:
Sample -,t/v,:,l: Lab File ID: 4U06008C: 1 ·.::=-
Level: .D~te Re,:ei ved: OE.IO:/·?o
% Moisture: not dee. de0:. Date E:<tra,:ted: 07 /O:/·?O
(SepF /C,:,nt /S,::in,:) :.30NC Date Analy=ed: {)7 /05/'j()
GF'C Cleanup: (Y/N.l t:J.._ pH: 4. 7 Diluti,:,n F"a,:t,:,r: 1.00 ~=--
CAS NO. COMPOUND
(OIKENTF:\TION UNITS:
~ug/L or ug/Kg) UG/VG
2100 83-3~-9---------A,:en~pf,tf,ene _________________ : 430
51-:8-5---------2,4-Di~itr,)pficnol ____________ : :21 (11)
100-0:-7--------4-Nitropfien,Jl ________________ : :2100
13:-64-9--------Diben=ofuran ________________ _ 430
1:1-14-:--------2,4-Dinitrotoluene ___________ : 430
84-66-:---------Diett,ylpf,tt,alate _____________ : 430
7005-72-3-------4-C,,1,Jr,)pt1enyl-p,1enylett1er ___ : 430 86-73-7---------Fluorene ____________________ _ 430
100-10-6--------4-Nitroaniline ______________ _ ::100
534-5~-t--------4,6-Dinitro-~-Met!1ylp•1en~l ___ : ~100
86-80-6---------N-Nitrosodipt,enylamine (!) ___ : 430
101-55-3--------4-Br,,mop,,eny!-pJ,enylether ____ : 430 118-74-1--------Hexact,lorobenzene ___________ _ 430
87-86-5---------Pent~chl,~r•)pt,enol ____________ : :21 ()c)
85-01-8---------PhenantJ,rene ________________ _ 430 120-12-7--------Anthr~cene __________________ _ 430
B4-74-2---------Di-n-Butylphthalate __________ : 430
206--44-0--------fluor,mthene :
12'ii-OO-O--------Pyrene ______ ::::::::::::::::::
430
430
B:3~B~7---------Butylben=ylp11thalate _________ : 430
'31 '-''!14-1---------3, 3' -Di 0:h l ,or0oben= id i ne _______ : B60
56-55-3---------Ben~ora,Ant,,racene __________ _ 430 :21B-01-'3--------Chrysene _____________________ : 430
117-Bl-7--------bi~(:2-Ethyl11e:<yl)Phthalate ___ : 430
117-84-0--------Dl-n-Dctyl Phthalate _________ : 4.30
:oS-99-~--------Ben:01b1Flu,)rant•1ene ________ _ 430
207-08-9--------BenzorJ.lFluorant•iene ________ _ 430
50-32-8---------0enlo(a)Pyrene _______________ : 430
193-39-5--------Indeno(l,2,3-cd)Pyrene _______ : 430
53-70-3---------0ibenz(a,h)Antt,racene ________ : 431)
191-24-2--------Benzo(g,h,i)Perylene _________ : 430
-------------
Q
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:u :u
-----(I) -Cannot be separated from Diphenylamine 000836
FORM I SV-2 1/87 Re·
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1 8
SEMIVOLATILE OF·i~ANICS AfJALYSIS DA~~ SHEET EPA SAMP _ _o NO
S-!3A-F:' :--1
Lab Name: KEYSTONE EN').
L2b ,::,:,de: fEYTX Case ,"J.:,.: c)E.(H)S SAS N,:,.:
M~tri~: (s,,il/water) SOIL L.ib Sompl e ID: ·j()(JE,1)081:
Lab File ID: .iuosoosc:;
Levo 1 : (low/med) =L~□~W~-Date, F·e,: ~i ·12d: OE,/0:1':10
:: Moisture: not dee. de,:. Date Extra,:ted: OE,/OE,/·30
6PC Cleanup: (YIN) r-J__ c;H: .j. 7 DilLttion ta,:t,:,r: 1.00
CAS NO. C 8t--:F·OLJND
CON,: ENT~:AT I ON Urt I TS:
(ug/L ,:,r ug/Kg) \JG/KG
!1:,8-35-2--------P~ien,,l _______________________ : 420
!!1-44-4--------bisf2-ChloroethyllEther ______ : 420
'35-57-8---·-·-7---:.::-Ch l ,:,r ,:,phen,:,l _______________ : 4:C>
541-73-1--------1,3-0ict,lor,Jben=ene __________ : 420
106-46-7--------1,4-Dict,loroben:ene __________ : 4:20
100-51-6--------Ben:yl Alco•iol _______________ : 420
~5-50-1---------t,:-Dichloroben:ene __________ : 420
95-48-7---------2-Methylphenol _______________ : 420
39638-3:-9------bisi:2-C}ilorois,,pr,,pyl)Ether __ : 4:2'0
!OE.-.J4-5--------4-Methylpf1enol _______________ : 420
621-64-7--------N-Nitro~o-Di-n-Propylamine ___ : 420
67-7:-1---------He~act,loroethane ____________ _ 420
98-95-3---------Nitr•~ben=ene ________________ _ 4:0
78-59-1---------Is,,ptiorone ___________________ : 4'20
88-75-5---------2-Nitropt,enol ________________ : 4:<)
105-E,7-9--------2,4-Dimethylphenol ___________ : 421)
65-85-0---------Ben.;:oic Acid ________________ _ 2100
11!-91-t--------bis(2-ChlaroethoxylMethane ___ : 420
120-83-2--------2,4-0i,:}1lorop•1enol ___________ : 4-ZO
120_-82-1--------1, :, 4-Tr i chl or ob en.;: ene _______ : 420 91-20-3---------Naphth~lene __________________ : 4:.:,1)
106-47-8--------4-Chlaroaniline _____________ _ 4'.:0
87-E,8-3---------Hc,xachlorabutadtene _________ _ 420
59-50-7---------4-Chlora-3-Methylphenol ______ : 420
9!-57-E,---------2-Methyln3phthalene __________ : 4:0
77-47-4---------Hexachlorocyclopentadiene ____ : 420
88-06-:---------2,4,6-Tri•;hloropt,enol ________ : 4:.:,0
95-95-4---------:,4,5-Trichloropt,enol ________ : 2100
'31-58-7---------2-Ch 1 c,r ,:,n.aphthal ene __________ : 4'.::0
88-74-4---------:-Nitroaniline _______________ : 2100
131-11-3--------Dimett,yl Pt,tt,alat~ ___________ : 4:20
208-9E,-8--------Acenaohthylene _______________ : 420
61)6-:0-2--------2,6-0initrotoluene ___________ : 420
:[]
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Q
~
FORM I SV-1 1/87 Re
00085~
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1i:
SEMIVOLATILE OF'GANl~E ANALYSIS DATA SHEE7
Veystone DC• OEOOS -04-
EPA SAMPLE MC
S-13A-F8r.:-c
Lab C ,:,de: ! EYTX Case N,:,.: Ob(H)S SAS N,:,.: SDl3 Ne,. : C30WA
Lmb S~mple ID: 900E00813
Sample 1.Jt /v,:,l: 30.0 (9/ml) ~ Lab File ID: 4LJ05008Cl:
Level: <" l ,:,•.J/med) LOW Date Re,:eived: 06/0:l~O
% M,:,isture: not dee. __ de,:. Date Extracted: OE/OE/80
Ext.r.J.1:t. i,:,n: ,·sepF/C,~nt/Sonc)
pH: 4.7 Di I ut i ,:,n Fa,:t,:,r: 1. 00
(:ONCENTF:AT I ON UN I TS:
CAS NO. COMPOUND 1: ug /L ,:ir ug /Kg) UGn·:G Q
2100 :c 83-3:-·~---------Acenaphtt,ene _________________ : 420 :u
51-:8-5----------:,4-Dinitropt,cn,)l ____________ : 2100 :u 1()0-02-7--------4-Nitrop!ienol ________________ :· 211)1) :u t3~-64-~--------01ben:,)furan ________________ _ 4:0 :u 1~1-14-:--------2,4-Dinitrotoluene ___________ : .. r:o :u
84-66-2---------Dietl,y!phth~late _____________ : 4:0 :u
7005-7:-3-------4-Chlorophenyl-p•ienylet•ier ___ : 42'0 :u 86-7:-7---------Fluorene ____________________ _ 4-.,::r) :u 100-10-6--------.i-N1troan1l1ne ______________ _ 2100 :u
534-5:-1--------4,6-0initro-2-Methylphenol ___ : 2100 :u
86-31)-6---------N-Nitrosodipt,enylamine (l) ___ : 420 :u
11)1-55-3--------4-Bromophenyl-pt,enylether ____ : 420 :u
118-74-1--------Hexachloroben:ene ___________ _ 420 :u
87-86-5---------Pentachl•~ropt,onol ____________ : 210<) :u 85-01-8---------Phenanthrene ________________ _ 4:0 :u 1~0-12-7--------Anthracene __________________ _ 420 :u
84-74-2---------Di-n-Butylphthalate __________ : 420 :u
206-44-0--------FI uor ant hene : 420 :u
lz<l.~0-0--------Pyrene _______________________ :
85..;68-7---------Butyl ben: y I pl1thal ate _________ :
420 :u
420 :u
91~g4-1---------3,3'-Dichloroben=idine _______ : 850 :u
56-55-3---------Benzo(a)Antliracene ___________ : 420 :u
218-01-9--------Chrysene _____________________ : 420 :u
117-81-7--------bis(2-Ethyl11~xy!JPhthalate ___ : 4:0 :u
117-84-0--------Di-n-Octyl Phthalate _________ : 420 :u
:1)5-99-2--------0un~o<blFluor~nt•iene ________ _ 420 :u
207-08-3--------Ben:o(k)Fluoranttiene _________ : 420 :u 50-3:-8---------Benz~(a)Pyrene _______________ : 420 :u
193-39-5--------Indeno<l,2,3-cd)Pyrene _______ : 4:0 :u
53-70-3---------Dibenz(a,h)Antbra~ene ________ : 420 :u
181-24-2--------Ben:olg,h,i)Perylene _________ : 420 :u
000855
FORM I SV-2 1 /87 Re
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18
SEM!VOLATILE ORGANICS ANALYSIS DATA SHEET
l'.ey3t,one DC• 06008 -)4-
_EPA SAMPL:c NO.
S-80
SAS N,o.: SDG No.: C30WI-
Matrix: (s,)il/water) SOIL L.c\b Sample ID: ·::iOOE,i)c)S<)~
Sample wt /v,:,l: 30.0 fg/ml) §__ Lab Fi 1 e ID: ~ UOE.OOBCC,::
L2vel: Clow/medl =L~O~W __ Date, F.:e,: e i ved: 01:../01 /':IC
:: M,:,i st ur e: n,:,t de,:. ___!_2 de,:. Date E:,;tra,:ted: 0£/06/'30
(SepF/C,)nt/S,)nc)
pH: 5.4
Date Analy:ad: 1)6/19/31)
Dilution Fa(tor: 1.00
CON(HITF:A TI ON UN I TS:
,:,;5 NO. COMFOUND Cug/L or ug/Kg) UG,·~:G C!
108-35-~--------P•,en,)l ______________________ _
I 11--14-4--------bis I :::-Ch 1 ,:,r ,oet h y I J Et her _____ _
1'300 l. 370 :u 35-57-S---------2-c·t1lorc,pf1cnol _______________ : a:o
541-73-1--------l.3-Dicf1loroben:ene _________ _ 370 :u
11)E.-46-7--------1,4-Di(f1lorobon:ene __________ : 370 :u 100-51-£--------Ben=yl Alcohol _______________ : 370 :u
35-50-1---------1.~-01,:t,lor,,ben:one _________ _ 370 :u 95-48-7---------2-Methylphenol _______________ : 370 :u
3963S-3:-9------bisC2-Ct1l0r,,is0propyl)Ett1or __ : 37(1 :u 10£-44-5--------4-Methy!pl,eno! _______________ : 1 "300
6:1-64-7--------N-Nitrcs,~-Di-n-Propylamine ___ : 370 :u 67-7:-1---------Hexachlor,,ett,ane ____________ _ 370 :u 98-95-3---------Nitroben:ene ________________ _ 370 :u 78-59-1---------Isophorone ___________________ : 680 88-75-5---------2-Nitrophenol ________________ : 370 :u
105-67-9--------2,4-Dimethy!phenol ___________ : 370 :u 65-85-0---------Ben~oic Acid ________________ _ 1800 :u
l!l-91-1--------bisl:::-,:hlcraethoxylMethane ___ : 370 :u 120-83-2--------2,4-Dichl,)r,)pt,enol ___________ : 370 :u
120~82-1--------1,~,4-Trichloroben:ene _______ : 370 :u 91-20-3---------Naphthalenc __________________ : 370 :u 106~47-8--------4-Chloroan1!1ne _____________ _ 370 :u
87-68-3---------Hexachlorobutadi~ne _________ _ 370 :u
59-50-7---------4-Chlcro-J-Methylphenol ______ : 370 :u
91-57-6---------2-Metl1ylnap ►1tt1alene __________ : 370 :u
77-47-4---------He~achlorocy(l•)pentadiene ____ : 37fl :u
88-06-:---------2,4,6-Tri(l1l,,r0ph~nol ________ : 370 :u
'35-':15-4---------2, 4, 5-T r i ,: h l ,:,r ,:,phen,:,l ________ : 1800 :u
')1-58-7---------2-Chloron.1pt1t ►1.ll-?ne __________ : 37() :u 88-74-4---------2-Nitr•jdniline _______________ : 1800 :u
131-11-3--------Di methyl r-·h t ha l .1 t e ___________ : 12()() 208-96-8--------Acenaphthylene _______________ :
606-~0-2--------2,6-0initrotoluene ___________ :
370 :u
370 :u
------------------FORM I SV-1 1/87
000877
Re'.
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1C
SEMl'/OLATILE OF'C,ANI•:S 1\NAL'!SIS DA,A SIJEET EPA SAMF':_!,'. W
5-81)
Lab ,:,:,de: IEYTY Case N,:,.: 06t)08
Matrix: (s,~i!/water) SOIL
Sample wt/v,,l: 30.0 C:g/ml) §__ Lab File ID: 4UOE.OOS1~(·5
Level: 11,:""'/mc,d) LOW
7. M,:,isture: n,:,t. de,:. _1Q de,:, Date E~tra,:ted: 06/06/90
Ext r .3,: ti ,:,n: SOMC Date Anal;ced: 06/19/90
6F'C Cleanup: pH: 5.4 Dilution Fa(tor: 1.00
,:;.s NO. COMF'OUND
COM:: SNTF:A TI ON IJN I TS:
(ug/L or ug/Kg> UG/KG
1800
83-3:-9---------Acenaphtt,ene _________________ : 800 51-~8-5---------2,4-Dinitr,:,pt,en,)l ____________ : 750
100-0:-7--------4-Nitropl,enol ________________ : 1800 132-64-9--------Dibcnz,)furan _________________ : 370
1:1-14-:--------2,4-Dinitrotoluene ___________ : 370
84-66-2---------Diethylphth~lata _____________ : 371)
7005-72-3-------4-Cl,lorophenyl-pfienylether ___ : 371) 86-73-7---------Pluorene ____________________ _ 37(1
100-10-6--------4-N1troan1l1ne ______________ _ 1800
534-52-1--------4,6-0initro-2-M~tt,ylphenol ___ : 130(1
86-31)-6---------N-Nitrosodipheny!amine (I) ___ : 370
101-55-3--------4-Bromophenyl-phenylether ____ : 370 118-74-1--------Hexachloroben=ene ____________ : 370
87-86-S---------Pentachlor0phenol ____________ : 2501)
85-01-8---------Phenanthrene ________________ _ 1400
120-12-7--------Anthracene __________________ _ 370
84-74-2---------Di-n-Butylphthalate __________ : 370
20&-44-0--------Fluoranthene _________________ : 370
129~00-0--------Pyrene _______________________ : 1600
85--68-7---------Butylbencylphtha!.:ite _________ : 37c)
91-g4-1 ---------3, 3' -Di,: h 1 ,:ir c,ben= i dine _______ : 730
5&-55-3---------BeAao(alAnthr.:icene __________ _ 370 218-01-9--------Chrysane _____________________ : 370
117-81-7--------bisl2-Ethylhe~yllPhthalate ___ : 371)
117-84-0--------Di-n-Octyl Phthalate _________ : 370
:o5-9~-~--------Ben:o(b)~luorant•1ene _________ : ltSOO
.207-J"JB-·3--------Ben:.J < I , F"l w:·,r anthene ________ _ 370
50-3:-8---------Ben:o(a)Pyrenc _______________ : 371)
193-33-5--------Indeno(l,2,3-cd)Pyrene _______ : 370
53-70-3---------Diben=(a,h)Anthracene ________ : 370
191-:4-2--------BenzoCg,h,i)Perylene _________ : 1400
:u
:J :u :u :u
:u :u
:u :u
:u :u
:u :u
:u
:u :u
:u :u :u :u :u :u
:u
:u
:u
:u
(I) -Cannot be separated from Diphenylamine
F"ORl1 I SV-2 000878
Q
l /87 Re
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Keyston~ DC~ 06c)OE -,)4-
Lab S.Jmp:e ID:
Lab Fi 1 e : D: 4U06(H)8C: :'
<low/med) L-□~W~-
de•:.
Dai:2 ,-\nz;l y:e,_J:
Dilution Fdct,~r: 1.()1) '-'-=--
1:0~JC:ENTRATION UNITS:
CJMF'GL'NC-•: •_tg/L ,:,r Ltg/;::g.! U•~/tC::1.3 Q
1 OB-·;.5-~--------Fh>:?n•:1 l ______________________ _ 410 : tJ
111-44-4--------bis.(2-C"hloroett,yl:•Ett,er ______ : "\ 10 :u
95-37-S----------2-Ct1l,~r,~pt1enol ________________ : 410 :u
541-73-l--------1.3-D1chloroben:ene _________ _ 41 ,) :u
11:•6-4~-7--------1,4-Dichloroben:ene __________ : ~i l i) :u
100-51-6--------Ben=yl Al,:ohol ______________ _ 410 :u
9~-5,~-l---------!,2-D1~t1l,;,r,,ben=~G~----------.:.:.10 :u
95-48-7---------:-Methylphenol ________________ : 4:) :u
3·~63S-3:-·3------bis(·2-ct,lc,r0is,)pr,:,pyl)Etl1er __ : -~ 1 t) :u
106-44-5--------4-Methylpt,enol _______________ : 41 (> :u
621-64-7--------N-Nitroso-Di-n-Propylamine ___ : 4 t 0 :u
67-7~-l---------He~achloroetf,ane ____________ _ 4 ~ ,~, :u
38-95-3---------Nitr,:iben:ene ________________ _ 4 l(l :u
79-59-1---------!sopf,orone ___________________ : 4 1 (l :u
88-75-5---------2-Nitrophen•Jl ________________ : 410 :u
105-67-9--------2,4-0imett1ylpf1enol ___________ : 4 l (I :u
65-85-0---------Benzoic Acid ________________ _ 21)(H) :u
111-91-1---~----bis(:-Cl1loroett1oxyJMetf1ane ___ : 410 :u
12Q.~83-2--------2, 4-0i ,: h 1 ,:ir ,:,phen,:.l ___________ :
12~82-1--------1, :, 4-Tr 1 ,: h 1 ,:ir ,:,benzene _______ :
41 (I :u
·HO :u
·31-20-3---------Naof,t. f,.3 I ene _________________ _ 411) :u
106:47-8--------4-Chloroaniline ______________ : 410 :u
87-68-3---------H~xachlorobutadiene _________ _ 410 :u
59-50-7---------4-Chloro-3-Mett,ylpt,enol ______ : 410 :u
91-57-6---------2-Methyln.:\ohth~lanc _________ _ 410 :u
77-4 7-4---------He:.:a,: h l ,.::,r ,.: .. : y,: ! ,:,per.tad i ent:? _____ : 41 ,:, :u
88-(=1E.-·2----------2 ~ 4, E,-:" r-:. ,: h 1-:,r ,:,phon,:,l ----·----: 41 (i : I J
35-95-4---------2,4,5-Trict1loropl1enol ________ : :21)(10 :u
'? ~ -58-7---------:.2-Ch l ,:,r ,:,n-lp ht ha l 2n,~ __________ : 4 l (i :u
88-74-4---------2-NitYoani!ine ______________ _ :20()0 :u
131-11-3--------Dimett,yl P•1thalate ___________ : ·:lo 1 t) :u
208-96-8--------Acenaphthylene _______________ : 410 :u
606-20-:--------2,6-Dinitrotoluene ___________ : 410 :u
----------------------------------------------------------------FORM I SV-1 1/87 Re,
000921
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1C
de,:. Date E~tracted: 06/11/90
:30N(
:JFC C!eanup: 3. 7 Dilution F~ctor:
CG,"':F'GUND
CONCENTPATION UNITS:
!.ug,'L ,:,r Ltg/Kg) ~
21)00
83-32-9---------Acenaphtt,ene _________________ : 410
51-:8-5----------~,-·i-Cinitr,~pr1en,~: ____________ ; -::o,)O
101)-1):2-7--------4-Ni tr ,:,phen,:,l ________________ : :::ooo
tJ:-64-3--------Dibenzofur~n _________________ _ -~ 10
121-14-2--------:.4-D,nitrotoluene __________ _ 410
41 (J
41 !)
41 (i
.::1)00
534-5~-1--------4,6-Oinitro-~-Met•iylphenol ___ : ::ooo
86-30-6---------N-Nitros0dip•1enyl~mine c·:) ___ : 410
101-55-3--------4-Brc,mop•,cnyl-ot,enylother ____ : 410
118-74-1--------Hexact,!aroben~ene ___________ _ 410
87-96-5---------Fentac>1loropt1enol ____________ : -.::ooo
65-1J1-8---------Phenant•1rene ________________ _ 410
120-1:-7--------Anthracene __________________ _ 410
84-74-2---------Di-n-Butylphthalate __________ : 410
.206-44-0--------Fl u,:,r anthene ________________ _ 410
12g.:.OO-O--------Pyrene _______________________ : 410
85-'68-7---------But yl b•an.: y l pl1 th,,J .,te _________ I 410
'31-94-1---------3, 3' -Di ,:h l c,r ,:,benz i dine _______ : 820
56-55-3---------Benzo<aJAntt,racene __________ _ 410
218-01-9--------Chrysene _____________________ : 410
117-81-7--------bis(2-Ethylhexy!JPhthalate ___ : 2500
117-8-l-O--------Di-n-Octyl P~1thal3t2 __________ : 410
::os -·:r:1-:: --------82r:: ,:, , b , :--~ · 1•:•r Jn i, tl,.=r.e ________ _ 410
.::o7-1)8-'3--------8en:.,:,, : , Fl L11:1r :1n t hene ________ _ 410
50-3:-8---------Ben:,)(J)Pyrenc _______________ : 410
1~3-33-5--------Indeno(l,2,3-cd)F·yrene _______ : 410
53-70-3---------Diben:(d,t1jAnt ►1racene ________ : ·HO
191-24-2--------Ben:.o(g,h,i)Perylene _________ : 410
1, (H)
' J:,
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:u :u
:u
:u :u
:u :u
:u
:u
:u
:u :u :u :u :u
:u
:u
:u :u
:u :u
:u :u
:u :u :u :u
:u
:u :u
-----------------------------------------------------------(1) -Cannot be separated from Oiphenylamine 000922
FORM I SV-2 1/87 Re·
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SAS N,:,. :
3(). () Lab Fi!e ID:
LCl✓ Oat e F:e,:ei ved:
de,:.
·3c,·~1:
6.=·c C: ea.nup: i y /i'-J.1 N Dilution Fact,:.r: ~1~-~(•~C_, __
·: 2~iC'.::i·J"ir.::~ T: O~J U~J I T3:
iuy/L .:,r :_19/i<g) U13/f<§,
410
111-44-,t--------bis(2-Cf1l,,roethyl)Ether _____ _ 410
41 (J
541-73-1--------1,3-Dict1l,~roben:en~ __________ : 4 1 (I
106-46-7--------1,4-D1,:•1loroben:ene _________ _ 410
1<)0-51-6--------Ben:yl Alcohol _______________ : 4 10
·3S-5(l-l---------1.:-Di,:hl,)rooen:ene _________ _ i 1 C
35-48-7---------2-Mett,ylphenol _______________ : 41 (J
33638-32-·~-------bi31·2-Cfil,,roisopr,,pyl)Etf1er __ : 410
l 1)~-44-5--------4-~1etf11lpl1enol _______________ · 41 !)
6:l-64·-7--------N-Nitr•)SO-Di-n-F·rc,pylamine ___ : 410
;7-;:-1---------Hexacf1loroethane ____________ _ ..j. 1 (l
98-'35-3---------Nitroben:ene ________________ _ 4 1 I)
78-59-1---------Isop>,orone ___________________ : 410
88-75-5---------2-Nitropt,enol ________________ : 410
105-67-3--------2,4-0imethylpfienol ___________ : 410
6~-85-0---------Benzoic A~id _________________ : 2()1)1)
111-91-1--------bis(2-Chloroethoxy)Methane ___ : 410
120-83-2--------~,4-0ichlorc,phenol ___________ : 410
120~02-1--------1,:,4-Trict,l,)roben:ene _______ : 410
'31-~0-3---------Napt,thal~ne __________________ : E,8
106~47-S--------4-Chl0roan1!1ne _____________ _ 410
87-68-3---------H~xachlorobutadiene 410
59-50-7---------4-Ch!oro-3-Methylp/1enol ______ : 410
91-57-6---------:-Methvlnaohthalene _________ _ 410
77-·~ 7 -·l---------He :,.· a,: h l ,:,r ,:,c,1,: 1 c,o ent ad i ene 410
88-•~~-2---------~,4~6-Tricf1l0r,:,pt1enol ________ : 410
35-9S-•t---------2,4,5-Trichloropt1enol ________ : :.::ooo
Jl-58-7---------1-Ct,loron~pt,th~lene __________ : 410
88-7~-4---------:-N1troan1l1ne ______________ _ 2000
131-11-3--------Dimethyl Phtha!ate ___________ : 410
208-96-8--------Acenaptithylene _______________ : 410
61)6-~0-2--------2,6-Dinitrotoluene ___________ : 410
0
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--------------------------------------------------------------·--FORM I SV-1 1/87 Re·
000943
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~eystone C(ij 0601)8 -•:•J-
L_,b 2~1,T,Cl2 !D:
:_ab Fi 1 e ID: -4U0f.(lc)8C:...:
de,:.
5. 1 Dilution Factor: ~l~-~oJ,:_, __
1:'Jr~CENTF:,·'\T:Ot·: UNITS:
i"t...·.9/L ,:,r" L.19,'L:9) 1J1::i·:~.:1::i
·:;1·?-•)·j-·.::------- --3-~li t ,-,:,,3n i 1 i ni:: ______________ _ :2000
83-3:::-·?----------M,: enaph t he-r,e _________________ : 410
51-22-5----------2,4-Dinitr,)o•1cn,,l ____________ : °2(H)()
11:•o-1:l:::-7--------4-Nitrophenol ________________ : 2000
13:::-64-~--------Diben:ofur.an ________________ _ 411)
1:21-14-:--------:::,4-D1n1trotolLt~ne ___________ : 410
84-65-:::-------·--C:~t~·1lo•1tl1JlJte _____________ _ 41 (I
410
--i t '.)
:.:::•)(:,)
534-S:-1--------4,6-Dinitro-:-Mett1ylp/1en,,1 ___ : .::ooo
86-30-6---------N-Nitrosc,dipl1enylam1ne fl) ___ : •l 10
101-55-3--------4-8romopf1enyl-pf1enylether _____ : -11 I)
118-74-1--------He~achloroben=ene ___________ _ 410
87-86-5---------Pentachlorophenol ____________ : 461)
85-t)l-8---------Pt,enantt,rene ________________ _ ·:i·.:
1~0-12-7--------Anthracene __________________ _ 410
84-74-2---------Dl-n-Butylphthalate __________ : 410
206;44-0--------Fl uo::ir .J.nt hene ________________ _ 121)
129~00-0--------Pyrene _______________________ : ·34
85-68-7---------Butyl ben: y l pl1 t l1a I ate _________ : 4 l I)
31-94-1---------3,3'-01cf1l0rc,ben=idine _______ : 8:20
56-55-3---------8€nzota1Antf1racene __________ _ 411)
218-01-9--------Chrysene _____________________ : 410
l l 7-81-7--------bl s ( 2-Et hy l he:<y I ) F·hthal ate ___ : 130
117-'3,!-(J--------D1-n-O,:tyl F·hthal ate __________ : 410
2(iS -·3·~1-·2 --- -----8,:in= ,:, !. b :, '.··: i.1,:.r .. ,n t tH:n ~ _________ _ 41 (1
.:.c)7-<J8-'3--------Ben.:.:, t ~ i t-1 u,:,r ant hene ________ _ 4 1 ,:.
S0-32-8-------·--Benzo(d.,Pyrane _______________ : 4 1 (I
133-J1-5--------Indeno!·:,~,3-cd)Pyrene ________ : -t 1 (•
53·-7!)-3---------Dibenz(a,f1JAntt1ra~ene ________ : 4 I 1)
191-24-2--------Ben:0(9,h,1JPerylene _________ : 410
----------------------------------------------(1) -Cannot be separated from Diphenylamine
FORM I SV-2
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000944
1 /87 Re·
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18
SEMIVOLATILE ORGANICS' ANALYSIS DATA SHEET
Keystone DC# 06008 -04-1
_EPA SAMPLE NO.
X-45-WA
Lab Name: KEYSTONE ENV. C.:int r a,: t: 179~8(')-04
Lab C,ode: KEYTX Case No.: C6008 SAS N,o.: SDG N,:i.: C30WA
Matrix: (s,:,i I /.iater) 5011,__ Lab Sample ID: 9<)0E,0081_9 __
Sample .it/vol: 30.0 (g /mU §__ Lab File ID: 4UOE-0•)8C 19
Level: (I c,.i/med) LOW Date Rei: ei ved: 06/05/90
'l. M,:,isture: nc,t dee. 20 dee. Date Extra,: t ed: 05/07190
Extracti,:in: <SepF/Cont/Sonc) SONC Date Analyzed: 06/ I '3/90
GF'C CleanLtp: (Y/N) t:!_ pH: 4.5 Dilution Fa,:tor:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol ______________________ _ 820
111-44-4--------bisC2-ChloroethyllEther ______ : 820
95-57-8---------2-Chlorophenol _______________ : 820
541-73-1--------l,3-Dicl1loroben~ene __________ : 820
t1)6-46-7--------1,4-0i~~1lorobenzene __________ : 820
100-51-E,--------Ben:yl Alcohol _______________ : 820
35-50-1---------1,2-Di,hlorobenzene __________ : 820
95-48-7---------2-Methylphenol _______________ : 820
39638-32-9------bisC2-Chloroisopropyl)Ether __ : 820
106-44-5--------4-Methylphenol _______________ : 820
621-64-7--------N-Nitroso-Di-n-Propylamine ___ : 820
67-72-1---------Hexachloroethane ____________ _ 820
98-95-3---------Nitrobenzene ________________ _ 820 78-59-1---------Isophorone ___________________ : 820
88-75-5---------2-Nitrophenol ________________ : 820
!05-57-9--------2,4-Dimethylphenol ___________ : 820
65-85-0---------Benzo,c Acid ________________ _ 4000
lll-91-l--------bisl2-ChloroethoxylMethane __ _ 820
120-83-2--------2,4-Dichlorophenol __________ _ 820
120-82-1--------1,2,4-Trichlorobenzene ______ _ 820
91-20-3---------Naphthalene _________________ _ 820
106-47-8--------4-Chloroaniline _____________ _ 820
87-68-3---------Hexachlorobutadiene _________ _ 820
59-:50-7-------4-Chloro-3-Methylphenol _____ _ 820
91-57-6---------2-Methylnaphthalene _________ _ 820
77-47-4---------Hexachlorocyc!opentadiene ___ _ 820
88-06-2---------2,4,6-Trichlorophenol _______ _ 820
95-95-4---------2,4,5-Trichlorophenol _______ _ 4000
91-58-7---------2-Chloronaphtha!ene _________ _ 820
88-74-4---------2-Nitroaniline ______________ _ 4000
131-11-3--------Dimethyl Phthalate __________ _ 820
208-96-8--------Acenaphthy!ene ______________ _ 820
606~20-2--------2,6-Dinitrotoluene __________ _ 820
FORM I SV-1
2.0
Q
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1 /87 Rev
000981
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IC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Keyst,:,nR DCI 06008 -04-
_EPA SAMPLE NO.
X-46-WA
Lab Name: KEYSTONE ENV. Contract: 179280-04
SAS No.:
--------------
Lab Code: KEYTX Case N,:,.: 06008 SDG No.: C30WA
Matrix: <soil/water) SOIL Lab Sample ID: 900600813
Sample wt /vol: 30.0 (g/mU G __ Lab File ID: 4U06008C:9
Level: ( l ,:,w/med) LOW Date Received: 06/06/90
I. Mc,i sture: not de,:. 20 dee. Date Extracted: 06/07/90
Extra,: ti ,:in: (SepF/Cont/Sonc) SONC Date Analyzed: 06/ 19/'30
GPC Cleanup: (Y/N) ",!_ pH: 4.5 Dilution Factor:
CAS NO. COMPOUND
CONCENTRATION UNITS:
( ug/L ,:,r ug /Kg l UG/KG
99-09-2---------3-Nitroaniline ______________ _ 4000
83-3:-9---------Acenaphthene ________________ _ 820
51-28-5---------2,4-Dinitrophenol ___________ _ 4000 100-02-7--------4-Nitrophenol _______________ _ 4000
132-64-9--------Dibenzofuran ________________ _ 820
121-14-2--------2,4-Dinitrotoluene __________ _ 820
84-66-2---------Diethylphthalate ____________ _ 820
7005-72-3-------4-Chlorophenyl-phenylether ___ , 820 86-73-7---------Fluorene ____________________ _ 820 100-10-6--------4-Nitroaniline ______________ _ 4000
534-52-1--------4,6-Dinitro-2-Methylphenol ___ : 4000
86-30-6---------N-Nitrosodiphenylamine (1l ___ : 820
101-55-3--------4-Bromophenyl-phenylether ____ : 820
118-74-1--------Hexachlorobenzene ___________ _ 820 87-86-5---------Pentachlorophenol ____________ : 4000
85-01-8---------Phenanthrene ________________ _ 820 120-12-7--------Anthracene __________________ _ 820
84-74-2---------Dl-n-Butylphthalate __________ , 820 206-44-0--------,luoranthene ________________ _ 820
129-00-0-------Pyrene ______________________ _ 820
85-68-7---------Butylbenzylphthalate ________ _ 820
'91~~-1--------3,3'-Dichlorobenzidine ______ _ 1600
56-55-3---------Benzo(alAnthracene __________ _ 820
218-01-9--------Chrysene _____________________ , 820
117-81-7--------bis(2-EthylhexyllPhthalate ___ : 1200
117-84-0--------Di-n-Octyl Phthalate ________ : 820
205-99-2--------Benzo(blrluoranthene ________ _ 820
207-08-9--------Benzo(klFluoranthene _______ _ 820
50-32-8---------Benzo(alPyrene ______________ _ 820
193-39-5--------Indeno<l,2,3-cdlPyrene _____ _ 820
53-70-3---------Dibenz(a,hlAnthracene _______ _ 820
191-24-2--------Benzo<g,h,ilPerylene 820
2.0
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FORM I SV-2 oop/~~~e-
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1B
SEMIVOLATILE OPGANICS ANALYSIS DATA SHEET
Keystone DCI 06008 -04-
_EPA SAMPLE NO.
X-7-LF'
Lab Name: KEYSTONE ENV. Contract: 179280-04
Lab Code: KEYTX Case No.: 06008 SAS No.: SDG No.: C30WA
Matrix: (sci I/water) SOIL Lab Sample ID: '3006ooe1e
Sample -,t/vol: 30.0 <glmU §__ Lab F'i I e ID: 4U06008C:9A
Level: (I .,., /med) LOW Date Re1:ei ved: 06/06/90
'l. Mcisture: not dee. 23 dee. Date Extracted: 06/07/90
Ex:tra,:tion: (SepF'/Cont/Sonc) SONC Date Analyzed: 06/26/90
GPC Cleanup: <YIN) ~ pH: 3.8 Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND <ug/L or ug/Kg) UG/KG 0
108-95-2--------Phenol ______________________ _ 430 u
lll-44-4--------bis(2-Chloroethyl)Ether ______ : 430 u
95-57-8---------2-Chloropfienol _______________ : 430 u
541-73-1--------1,3-Dichloroben:ene __________ : 430 u-
106-46-7--------1,4-Dichlor,obenzene __________ : 430 u 100-51-6--------Ben=yl Alcohol _______________ : 430 u
95-50-1---------1,2-Dichlorobenzene __________ : 430 u
95-48-7---------2-Methylphenol _______________ : 430 u
39638-32-9------bis(2-Chloroisopropyl)Ether __ : 430 u 106-44-5--------4-Methylphenol _______________ : 430 :u
621-64-7--------N-Nitroso-Di-n-Propylamine ___ : 430 :u
67-72-1---------Hexachloroethane ____________ _ 430 :u 98-95-3---------Nitrobenzene ________________ _ 430 :u
78-59-1---------Isophorone ___________________ : 430 :u 88-75-5---------2-Nitrophenol ________________ : 430 :u
105-67-9--------2,4-Dimethylphenol ___________ : 430 :u 65-85-0---------Benzoic Acid ________________ _ 2100 :u
111-9!-!--------bisC2-Chloroethoxy)Methane ___ : 430 :u
120-83-2--------2,4-Dichlorophenol ___________ • 430 :u
120-82-1--------1,2,4-Trichlorobenzene ______ _ 430 :u 91-20-3---------Naphthalene _________________ _ 430 . :u
1 ~-7-8-----4-Chl or oan i l i ne _____________ _
87,8-3---------Hexachlorobutadiene
'1 ----------59-®-7-----4-Ch l or o-3-Met hyl phenol _____ _
91~~7-6--------2-Methylnaphthalene _________ _
430 :u
430 :u
430 :u
430 :u
77-47-4-------Hexachlorocyclopentadiene ____ , 430 :u
88-06-2--------2,4,6-Trichlorophenol ________ : 430 :u
95-95-4---------2,4,5-Trichlorophenol ________ l 2100 u
91-58-7---------2-Chloronaphthalene __________ : 430 u
88-74-4---------2-Nitroaniline _______________ : 2100 u
131-11-3--------Dimethyl Phthalate ___________ l 430 u 208-96-8--------Acenaphthylene _______________ : 430 u
606-20-2--------2,6-Dinitrotoluene ___________ : 430 u :·
• • , _____________________________________________ 1 ____________ _
F'ORM I SV-1 1/87 Re,
001011
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IC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Key5tone DCI 06008 -0-C-,
_EPA SAMPLE 'IC.
Lab Name: KEYSTONE ENV,
Lab Code: KEY TX Case N,~.: OE.008
Matrix: (soil/water) SOIL
Contract: 179280-04
SAS No.:
Lab Sample
X-7-LF'
SDG No.: C30WA
ID: 900600818
Sample wt /v,:,l: 30.0 Cg/mU G __ Lab F'i le ID: 4U06008C 1 8A
Level: (low/med) LOW Date Re,:ei ved: 06/06/90
'l. M,::ii st ur e: not dee. ~ dee, Date Extracted: 06/07/90
E:-.traction: (Sepf' /Cont /S,~nc J SONG Date Analyzed: OE./26/90
GPC Cleanup: CY/NJ ~ pH: 3.8 Dilution F'actor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND <ug/L or ug/Kgl UG/KG Q
33-09-2---------3-Nitroaniline ______________ _
83-3:-9---------Acenaphthene ________________ _
51-28-5---------2,4-Dinitrophenol ___________ _
2100 u.
430 I.J:
2100 Ii
100-02-7--------4-Nitrophenol _______________ _ 2100 IJ
132-64-9--------Diben:ofuran ________________ _ 430 u
121-14-2--------2,4-Dinitrotoluene __________ _ 430 u
84-6€.-2---------Diethylphthalate ____________ _ 430 u
7005-72-3-------4-Chlorophenyl-phenylether __ _ 430 u 86-73-7---------F'luorene ____________________ _ 430 u
100-10-6--------4-Nitroan,line ______________ _ 2100 u
534-52-1--------4,6-Dinitro-2-Methylphenol ___ : 2100 u
8€.-30-6---------N-Nitrosodiphenylamine (!) __ _ 430 u
101-55-3--------4-Bromophenyl-phenylether ___ _ 430 u
118-74-1--------Hexachlorobenzene ___________ _ 430 .u
87-86-5---------Pentachlorophenol ___________ _ 2100 :u
85-01-8---------Phenanthrene ________________ _ 430 u
120-12-7--------Anthracene __________________ _ 430 u
84-74-2---------Di-n-Butylphthalate _________ _ 430 u
206-44-0--------F'luoranthene ________________ _ 430 u 129-00-0--~-----Pyrene _______________________ ,
• 85-68-7-~~------Butylbenzylphthalate ________ _
91-d<i-1--------3,3'-Dichlorobenzidin• ______ _
56-~-3---------Benzo(a)Anthracene
430 u
430 u
860 ·u
430 u 218;-,01-9-----1:Chrysene ____________________ _ 430 u
117-81-7--------bisC2-Ethylhexyl>Phthalate __ _ 1000 B
117-84-0-------Di-n-Octyl Phthalat•---------430 u
205-99-2--------Benzo(b)F'luoranthene ________ _ 430 u
207-08-9--------Benzo(k)F'luoranthena _____ _ 430 u
50-32-8---------Benzo<a>Pyrene _____________ _ 430 .u
193-39-5--------Indeno<l,2,3-cd)Pyrena _____ _ 430 :u
53-70-3---------Dibenz(a,h)Anthracena _______ _ 430 IU
191-24-2--------Benzo(g,h,i)Perylena _______ _ 430 :u
• :· '----------------------------------------------------------------.
(1) -Cannot be separated from Oiphenylamine 001012 r ..
fORl1 I SV-2 1/87 Re,
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1B
SEMIVOLATILE OPGANICS' ANALYSIS DATA SHEET
Keystone DCII 06008 -,."4-E
_EPA SAMPLE NO,
X-33
Lab Name: KEYSTONE ENV, Contract: 173280-04
SAS No,: Lab C,ode: KEYTX Case No.: 06008 SDG No.: C30WA
Matri:r:: (s,oi I /,.,ater J SOIL Lab Sample ID: 300600827
Sample wt /vol : 30.0 (g/ml) G __ Lab f"i 1 e ID: 4U06008C:27
Level: ( 1 .,,., / med J LOW Date Received: 06/07/30
1/. M,:d sture: not dee. -1.Q dee. Date Extracted: 06/11/30
Extracti.:,n: (SepF/Cont/Sonc) SONC Date Analyzed: 06/13/30
GPC Cleanup: (Y /NJ !'!!_ pH: 6.3 Diluti,,n factor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kgl UG/KG Q
108-35-:2--------Phenol ______________________ _ 370 :u
111-44-4--------bis(2-Chloroethyl)Ether ______ : 370 :u:
35-57-8---------2-Chlorophenol _______________ : 370 :u
541-73-1--------1,3-Dichlorobenzene __________ : 370 :u
106-46-7--------1,4-Dichlorobenzene __________ : 370 :u
100-51-6--------Benzyl Alcohol _______________ : 370 :u
95-50-1---------1,2-0ichlor,,benzene __________ : 370 :u
95-48-7---------2-Methylphenol _______________ : 370 :u
33638-32-3------bis(2-ChloroisopropyllEther __ : 370 :u
106-44-5--------4-Methylphenol _______________ ; 370 :u
621-64-7--------N-Nitroso-Di-n-Propylamine ___ : 370 :u
67-72-1---------Hexachloroethane ____________ _ 370 :u 38-95-3---------Nitrobenzene ________________ _ 370 u 78-53-1---------lsophorone ___________________ ' 370 u
88-75-5---------2-Nitrophenol _______________ _ 370 u
105-67-9--------2,4-Dimethylphenol __________ _ 370 u 65-85-0---------Benzoic Acid ________________ _ 1800 u
111-91-1--------bis(2-Chloroethoxy)Methane __ _ 370 u
120-83-2--------2,4-Dichlorophenol __________ _ 370 u
120-82-1-------1,2,4-Trichlorobenzene ______ _ 370 u
91-20-3-------Naphthalene ________________ _ 370 u
106-417-8-------4-Chloroaniline _____________ _ 370 u
87-68-3---------Hexachlorobutadiene _________ _ 370 u
59-:50-7------4-Chloro-3-Methylphenol _____ _ 370 u
91-57-6--------2-Methylnaphthalene _________ _ 370 u
77-47-4-------Hexachlorocyclopentadiene ___ _ 370 u
88-06-2---------2,4,6-Trichlorophenol ______ _ 370 u
95-95-4--------2,4,5-Trichlorophenol _______ _ 1800 u
91-58-7---------2-Chloronaphthalene _________ _ 370 u
88-74-4--------2-Nitroaniline _______________ : 1800 u
131-11-3--------Dimethyl Phthalate ___________ : 370 u
208-96-8--------Acenaphthylene _______________ : 370 u
606-20-2--------2,6-Dinitrotoluene ___________ : 370 u
------------------FORM I SV-1 1/87 Rev
001029
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IC Keystone DCI 06008 -04-
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _EPA SAMPLE NO.
X-'33
Lab Name: KEYSTONE ENV. Contract: 17'3:B0-04
Lab C,:,de: KEYTX Case No.: OE,008 SAS N,:,.: SDG No.: C30WA
Lab Sample ID: '300600827
Matrix: <soil/water) SOIL
Sample wt/vol: 30.0 < g/mU §__ Lab File ID: 4U06008C:7
Level: ( 1 ow/med I LOW Date Received: 06/07/90
7. Moisture: not dee. _!Q dee. Date Extracted: 06/11/90
Extra,:ti,::in: (SepF/Cant/Sanc) SONC Date Analyzed: 06/13/90
Dilution Fact,:,r: ~'~-0~0~--
CONCENTRATION UNITS:
GPC Cleanup: (YIN) tL.. pH: 6.3
CAS NO. COMPOUND lug/Lor ug/Kgl UG/KG Q
99-09-2---------3-Nitroaniline ______________ _ 1800 :u
83-32-9---------Acenaphthene ________________ _ 370 :u·
51-28-5---------2,4-0initrophenol ___________ _ 1800 :u
100-02-7--------4-Nitraphenol _______________ _ 1800 :u
132-64-g--------Dibenzofuran ________________ _ 370 :u
121-14-:--------2,4-Dinitrotoluene __________ _ 370 :u
84-66-2---------Diethylphthalate ____________ _ 370 :u
7005-72-3-------4-Chlorophenyl-phenylether __ _ 370 :JJ
86-73-7---------Fluorene ____________________ _ 370 :u
100-10-6--------4-Nitroaniline ______________ _ 1800 :u
534-52-1--------4,6-Dinitro-2-Methylphenol ___ : 1800 :u
86-30-6---------N-Nitrosodiphenylamine (1) ___ : 370 :u
101-55-3--------4-Bromophenyl-phenylether ___ _ 370 :u
118-74-1--------Hexachlorobenzene ___________ _ 370 :u
87-86-5---------Pentachlorophenol ___________ _ 1800 :u
85-01-8---------Phenanthrene ________________ _ 370 :u
120-12-7--------Anthracene __________________ _ 370 'U
84-74-2---------Di-n-Butylphthalate _________ _ 370 u
206-44-0--------Fluoranthene ________________ _ 370 u
129-00-0--------Pyrene ______________________ _ 370 u
85-&8-7---------Butylbenzylphthalate ________ _ 370 u
91-94-1------3,3'-Dichlorobenzidine ______ _ 730 u
56-55-3---------Benzo(a)Anthracene __________ _ 370 u
218--01-9-------Chrysene ____________________ _ 370 u
117-81-7-------bisC2-EthylhexyllPhthalate ___ , 74 :J
117-84-0------Di-n-Octyl Phthalate _________ : 370 :u
205-99-2--------BenzoCb)Fluoranthene _________ l 370 :u
207-08-9--------BenzoCk)Fluoranthene ________ _ 370 u
50-32-8---------Benzo(a)Pyrene ______________ _ 370 u
193-39-5--------IndenoCl,2,3-cd)Pyrene ______ _ 370 u
53-70-3---------DibenzCa,h)Anthracene _______ _ 370 u
191-24-2--------Benzo<g,h,i)Perylene ________ _ 370 u
-----------------------------------------------------------
1) -Cannot be separated from Diphenylamine 001030
FORM I sv-2 l /87 R,
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1B
SEMIVOLATILE OPGANICS,ANALYSIS DATA SHEET
Keyst 0ne DC• 060<)8 -04-
_EPA SAMPLE NO.
X-94
Lab Name: KEYSTONE ENV. Contract: 179280-04
Lab C,:,de: KEYTX Case N,~.: 06008 SAS No.: SDG No.: C30WA
Matrix: (soil/,.,ater) SOIL Lab Sample ID: 900600828
Sample ,.,t /vol: 30.0 (g/mU G __ Lab File ID: 4U06008C2eA
Level: (!,ow/med) LOW Date Received: 06/07 /'30
1/. Moisture: not dee. __ 8 dee. Date Extracted: 06/11/90
E ::< t r act i on : (SepF /Cont /S,onc l SONC Date Analyzed: 06/26/90
GF'C Cleanup: (Y/Nl ~ pH: 5.7 Dilution F"a,:tor:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kgl UG/KG
108-95-2--------Phenol ______________________ _ 1400
111-44-4--------bis(2-Chloroethyl)Ether ______ : 360
35-57-8---------2-Chlorop~1enol _______________ : 200
541-73-1--------l,3~Dichloroben:ene __________ : 360
106-46-7--------1,4-Dichlorobenzene __________ : 360
100-51-6--------Benzyl Alcohol _______________ : 360
"35-50-1---------1, 2-Di ,:h 1 or obenz ene __________ : 360
95-48-7---------2-Methylphenol _______________ l 360
3'3638-32-'3------b is (2-Ch l ,:ir ci sopr opyl) Ether __ : 360
106-44-5--------4-Methylphenol _______________ : 1300
621-64-7--------N-Nitroso-Di-n-Propylamine __ _ 360
67-72-1---------Hexachloroethane ____________ _ 360
98-95-3---------Nitrobenzene ________________ _ 360 78-59-1---------lsophorone __________________ _ 430
88-75-5---------2-Nitrophenol _______________ _ 360
105-67-9--------2,4-Dimethylphenol __________ _ 360
65-85-0---------Senzoic Acid ________________ _ 1700
111-91-1--------bisC2-Chloroethoxy)Methane __ _ 360
120-83-2--------2,4-Dichlorophenol __________ _ 360
120-82-1------1,2,4-Trichlorobenzene ______ _ 360
91-20-3--------Naphthalene _________________ _ 360
106-47-8--------4-Chloroaniline _____________ _ 360
87-68-3---------He,achlorobutadiene _________ _ 360
59-:50-7--------4-Chloro-3-Methylphenol _____ _ 360
91-57-6---------2-Methylnaphthalene _________ _ 360
77-47-4--------Hexachlorocyclopentadiene ____ : 360
88-06-2---------2,4,6-Trichlorophenol ________ : 360
95-95-4---------2,4,5-Trichlorophenol ________ : 1700
91-58-7---------2-Chloronaphthalene __________ : 360
88-74-4---------2-Nitroaniline _____________ _ 1700
131-11-3--------Dimethyl Phthalate ___________ : 1000
208-96-8--------Acenaphthylene _______________ : 360
606-20-2--------2,6-Dinitrotoluene ___________ : 360
1.00
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IC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Keystone DC• 06008 -o4-E
_EPA SAMPLE '«J. _
X-94
Lab Name: KEYSTONE ENV, Contract: 179280-04
Lab C,,de: KEYTX Case No.: 05008 SAS No.: SDG No.: C30WA
Matri,: (soil/water) SOIL Lab Sample ID: 900600828
Sample l,,Jt /vc,l : 30.0 (g/mLI §_ Lab File ID: 4U06008C28A
Level: ( l ,,w/med I LOW Date Received: 06/07/90
'l. f''"h)isture: not de,:. __ 8 dee. Date Extracted: 05/11/90
Extra,: t i on : (SepF/Cont/Soncl SONC Date Analyzed: 05/25/90
Dilution Factor: ~1~-~0~0 __ GF·C Cleanup: (Y/NI ~ pH: 5.7
CAS NO. COMPOUND
CONCENTRATION UN I TS:
(ug/L or ug/Kgl UG/KG
99-09-2---------3-Nitroaniline ______________ _
83-32-9---------Acenaphthene ________________ _
51-28-5---------2,4-Dinitrophenol ___________ _
100-02-7--------4-Nitrophenol _______________ _
132-64-9--------Diben:ofuran ________________ _
121-14-:--------2,4-Dinitrotoluene __________ _
84-65-2---------Diethylphthalate _____________ :
7005-72-3-------4-Chlorophenyl-phenylether ___ :
86-73-7---------Fluorene _____________________ :
100-10-5--------4-Nitroaniline ______________ _
534-52-1--------4,6-Dinitro-2-Methylphenol ___ :
85-30-5---------N-Nitrosodiphenylamine (1) ___ :
101-55-3--------4-Bromophenyl-phenylether ____ :
118-74-1--------Hexachloroben:ene ____________ :
87-86-5---------Pentachlorophenol ____________ :
85-01-8---------Phenanthrene _________________ :
120-12-7--------Anthracene ___________________ :
84-74-2---------Di-n-Butylphthalate __________ :
205-44-0------~-Fluoranthene _________________ :
129-00-0--------Pyrene _______________________ :
85-68-7---------Butylbenzylphthalate _________ :
91-94-1---------3,3'-Dichlorobenzidine _______ :
56-55-3---------Benzo(aJAnthracene ___________ ,
218-01-9--------Chrysene ____________________ _
117-81-7--------bisC2-EthylhexyllPhthalate __ _
117-84-0--------Di-n-Octyl Phthalate ________ _
205-99-2--------Benzo(blFluoranthene ______ . __
207-08-9--------Benzo(klFluoranthene ________ _
50-32-8---------Benzo(alPyrene ______________ _
193-39-5--------Indeno(l,2,3-cd>Pyrene ______ _
53-70-3---------Dibenz(a,h)Anthracene _______ _
191-24-2--------Benzo(g,h,i)Perylene ________ _
' '
1700
540
1400
1700
360
360
360
360
360
1700
1700
360
360
350
1300
990
360
360
360
1200
350
720
360
360
360
360
1100
360
360
360
360
960
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(1) -Cannot be separated from Diphenylamine 001054
FORM I SV-2 1 /87 Re•
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13
SEMIVOLATILE OPG~NICS ~NALYSJS D~TA SHEET
L~b N~ma: VEYSTONE ENV,
Samp I e ""t /v,:,!: l(l(H) (g/mL~ t!.b__ Lab File ID:
Level: LOW Date F.'e,:ei·,ed:
% MoistLtre: not dee. de,:. Date E~tra~ted: 06/04/90
(Y/N) ~ pH:
COMF·ouim
6.0
CONCENTRATION UNITS:
rL1g/L ,:,r Ltg/Kg) UG/L
lt)S-95-:--------Pt,enol _______________________ _
111-44-4--------bis<:-ChloroethyllEther ______ :
35-57-8---------:-Chloropt,enol _______________ :
541-73-1--------1,3-01,:t,loroben:ene _________ _
t1)6-46-7--------t,4-Di,:t1l,,roben:ene __________ :
100-51-6--------Ben:yl Alc0t1ol _______________ :
95-50-1---------1,:-0i,:t1lor0ben:ene __________ :
35-48-7---------2-M2tf1ylpt1enol _______________ :
3'~638-3:-3------bi;r:-ct,t,,roisc,propyl)Ether __ :
11)6-44-5--------4-Mett,ylpfienol _______________ :
6:1-64-7--------N-Nitr,~30-0i-n-Pr0pylamine ___ :
£7-72-1---------He~a(f1lor,,ethane ____________ _
38-95-3---------Nitr,)ben=ene ________________ _
78-53-1---------Isophorone ___________________ :
88-75-5---------:-Nitrophenol ________________ :
105-67-9--------2,4-Dimett1ylpf1enol ___________ :
65-85-0---------Benzoi, A,id ________________ _
11!-91-l--------bis(2-Chloroetho•yJMethane ___ :
12o=aa-2--------2,4-0i(hlor,)pf1enol ___________ :
120~82-1--------1,:,4-Tri,t1lor,)ben=ene _______ :
91~20-3---------Naphthalene __________________ :
106~47-8--------4-Chloroan1J1ne _____________ _
87-68-3---------Hexa,t,torobutadiene _________ _
59-50-7---------4-Chloro-3-Methylphenol ______ :
91-57-6---------2-Methylnap>,thalene __________ :
77-47-4---------Hexa,hlorocyclopentadiene ____ :
88-1)6-~----------:,4,6-Tri,t1loropt1onol ________ :
95-95-4---------:,4,5-Trichloropt,enol _______ _
'31-58-7---------'..:-Ch 1,:ir ,:,nap ht h.:.l >~ne _________ _
88-74-4---------2-Nitroaniline ______________ _
131-11-3--------Dimethyl Phthal~te __________ _
208-96-8--------Acenaphthylene ______________ _
606-20-2--------2,6-Dinitrotoluene __________ _
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----------------------------------------------------------------FORM I SV-1 1 /87 Re 000681
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SEMI VOL.~ TI LE OF:•:.AN I ,:·5 Atl,,L 'ISIS o:, 7 ;, SHEET _ EPA SAMP!..~ NO.
S-F: I NSA ~
SAS l'J,:,. : SDG No. : C3t)W,:.
Lab Sample ID: ':10060081 ~
Lab File ID: .:1LJf)E,(H)8C: :,!,
Level: (low/med) L=O~W~_ Date Pe,: ei ved: l)E,/(1:::1·:si(,
:: Moisture: not dee. de,:. Date E:,. tr a,: ted: OE, I 1)..\ I ·31)
( ScpF /C,:,nt /S,:,n,:) CCNT l)E, I ::s / '3c)
(Y/N) ~ pH: E,. 0 Diluti,)n Factor: £1~-~0~--
(.,:.S NO. ,:QMF·OUND
cmJCENTF:,, TI ON UN I TS:
(ug/L ,:,r 1.19/L'.g'i U1;i/l:_
50
83-3:-9---------Acenapt,tt,ene _________________ : 1 ,)
51-28-5---------~,4-Dinitr0pt1enol ____________ : 50
101)-()2-7--------4-Nitropt,enol ________________ : 50
132-64-9--------Diben:ofur~n ________________ _ 10
1:t-14-~--------2,4-D1n1trotoluene __________ _ 1 0
34-66-2---------Diett,ylphtf,alate _____________ : 1 ,:i
7005-7~-3-------4-Ct1l,,r,,pt1enyl-phenylett1er ___ : 10
:3E,-73-7---------Fl 1J,:•r ene ____________________ _ 10
100-11)-6--------4-N1troan1l1ne ______________ _ 50
534-52-1--------4,6-Dinitr,)-:-Matt1ylpt1enol ___ : 51)
86-30-6---------N-Nitrosodipt,enylamine (ll ___ : 1!)
101-55-3--------4-Brom,)pf1enyl-pt1enylether ____ : 10
118-74-1--------Hexact1loroben:ene ___________ _ I 1)
87-86-5---------Pentachloropt,enol ____________ : 5()
85-01-8---------Phenantt,rene ________________ _ I 0
1:0-12-7--------Anthracene __________________ _ 10
84-74-2---------Di-n-Butylphthalate __________ : 10
206-44-0--------Fluoranthene ________________ _ I 0
129:=00-0--------Pyrene _______________________ : 10
85-~8-7---------Butylbenc'/lPhthalate _________ : 10
91-94-1---------3,3'-Dichlorobenzidine _______ : ::o
5E,-55-3---------Bencola)Anthracene __________ _ 10
218-01-9--------Chrysene _____________________ : 10
117-Bl-7--------bisl2-Ethyl11e,yllPhthalate ___ : -,
117-84-0--------Di-n-Octyl Phthalate _________ ! 10
:1)5-·?9-~--------Ben:01bJFlu,)r~ntt1ane ________ _ 10
~07-08-9--------Ben:oii )Fluoranthene ________ _ 10
50-32-8---------Ben:o(alPyrene _______________ : I I)
133-39-5--------Indenof!,2,3-cd)Pyrene _______ : 10
53-70-3---------0ibenz(d,ti)Antt,ra~~ne ________ : 10
191-24-2--------BenzoCg,h,i)Perylene _________ : 10
' ' ·----------------------------------------------· -------------(1) -Cannot be separated from Diphenylamine
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FORM I SV-2 000685 1/87 Re·
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SE:-11':C~ATILE OF:GANICS MJALYSIS DATA SHEET _EPA SAMPLE NO.
X-F·INSA7E
SAS N,:,. : SDG N,:,. : (30WA
L.3b ·3ample ID: ·:;4(H)E,(H)8 1 E.
1 (1()() Cg/ml) t1.b__ Lab File ID: -lLJl)E,<)()8(1':.
D.)t;e F:e,:eived:
% M,~isture: not dee. dee. Date E~tract2d: !)6/()4/30
pH: ..1, 5 Dilution Factor: ~1~-~0~--
COMFtJUND
CONCENTRATION UNITS:
(u9 .. L ,:,r :..ig/Kg) ~~,~ C!
tr)S-95-:--------Pt,~nol ______________________ _ 11) :u
lll-44-4--------tis1·2-Chlor(,ett1yl)Ett1er ______ : 10 :u
95-57--8---------:-1:ht,,ropt,en,~l __ · ____________ : 1 I) :u
541-73-1--------1,3-0ichlor,)ben:ene __________ : 10 ; IJ
106-46-7--------1,4-01ct1loroben:ene _________ _ 10 :u
100-51-6--------Ben:yl Alcohol _______________ : 10 :u
·1s-S,)-1---------1 , ..:--o 1 ,: h l ,:,r ,:,b en: ene ______ . __ _ t (l :u
~5-JS-7---------2-Methylchenol _______________ : 1 (I :u
3"?€J:S-3..::-·3------b i 3 c::-Ch 1 ,:,r ,:,i :;,:,pr,:,py l :i Et her __ : 10 :u
106-44-5--------4-Methylphenol _______________ : 10 :u
6~1-64-7--------N-Nitroso-Di-n-Pr~•pylamine ___ : !U :u
67-72-1---------Hexachloroett,ane ____________ _ l I} :u
38-~5-3---------Nitroben:ene ________________ _ 10 :u
78-53-1---------Isophorone ___________________ : 10 :u
88-75-5---------:-Nitrop►,enol ________________ : I<) :u
105-67-9--------2,4-Dimethylphenol ___________ : 1 I) :u
65-85-0---------Benzoic Acid ________________ _ 50 :u
111-91-1--------bis(2-Chloroetho,ylMethane ___ : 10 :u
120-'83-2--------2, 4-Di ch! ,,r ,:,phenol ___________ : 1 f) :u
120:.~2-1--------1,:, 4-Tr i ,:h l ,:,r ,:,ben= ene _______ :
91~~0-3---------Naphthalene __________________ :
10 :u
1 c) :u
1<)6,047-8--------4-Ch) ,,r ,:,an 1 I 1 ne _____________ _ I c) :u
87-68-3---------He,achlorobutadiene _________ _ I c) :u
59-50-7---------4-C11loro-3-Mett1ylpt1enol ______ : 11) :u
91-57-6---------2-Methylnaphthalene __________ : I c) :u
77-47-4---------He~achlorocyclooentadiene ____ : 10 :u
88-06-2---------2,4,6-Tri,:hl,:,r,,p•icn,,l ________ : .to :u
35-95-4---------2,4,5-Trict,Ioropt,enol ________ : 50 :u
91-58-7---------2-Chloronapl,tt,alena __________ : 1 I) :u
88-74-4---------:-N1troan1!1ne ______________ _ 50 :u
131-11-3--------Dimethyl Phthalate ___________ : 10 :u
208-96-8--------Acenaphthy!ene _______________ : 10 :u
606-20-2--------2,6-Dinitrotoluene ___________ : 10 :u
' ' '----------------------------------------------· FOF:M I SV-1 ------------------1/87
000695
Re,
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_EPA SAMPLE ,'JO.
X-RINS,HE
Lab ,::,:,de: l'EYTY SAS n:,.: SD(i No.: C20W~
Lab Sample ID: 300600816
S.?.mp 1 e \.Jt /v,:il : 1 ()1)(1 rg/ml) ~ Lab File IO: 4UOE.008C~:::
~ MoistL1re: not de~. Date E~tra~ted: OS/04/90
C.OMT
pH: 4.5 Di 1 u ti ,:,n F 3,: t ,:ir: t • o _,__,_"'----
CAS NO. ,:.QMF'DIJNO
,:□N(:ENTF'.AT I otl UN ITS:
··ug/L ,:,r ug/t~g) ~
33-,)3-2----------3-NitroJniline _______________ : 50
83-3:-9---------Acenapt,thene _________________ : 10
51-:G-5---------:,4-Dinit~,~pfien,,l ____________ : 50
100-0:-7--------4-Nitrc,phenol ________________ : 50
1J2-64-3--------D1bcn:0furan ________________ _ 10
1:1-t4-:--------:.4-D1n1trotoluene __________ _ 10
84-~6-:----------Diet•1ylp>1t ►,~l~te _____________ : 10
70()5-72-3-------4-Chlorophenyl-phenylet•ier ___ : 10
86-73-7---------F!u0r~ne ____________________ _ l f)
100-1 ()-6--------4-Nt tr ,:,an1 1 l ne ______________ _ 5('
534-52-1--------4,6-Dinitro-2-Met~iylpt,en,~l ___ : 5('
86-3()-6---------N-Nitrosodip!ienylamine (1) ___ : 1 r:~
101-55-3--------•I-Promopt,enyl-phenylett,er ____ : l 1)
118-74-1--------Hexactiloroben:ene ___________ _ 10
87-86-5---------Pentachlorophenol ____________ : 50
85-0t-8---------Pt1enantf1rene ________________ _ 10
1~0-1:-7--------Antt,racene __________________ _ 10
84-74-2---------Di-n-Butylphthalate __________ :
206~44-0--------Fluoranthene ________________ _
10
I 0
1:9~00-0--------Pyrene ________ ~ ______________ :
95,.;~-7---------Butylbenzylphthalate _________ :
10
10
91~4-1---------3, 3' -Di,: hl ,:,r ,:,ben: id i ne _______ : 20
56-55-3---------Benzo(a)Antt,racene ___________ : 10
218-01-9--------Chrysene _____________________ : Jc)
117-81-7--------bi s C2-Ett1y l hexy l) Phthal ate ___ : 1 C)
117-84-0--------Di-n-Octyl Phthalat~ _________ : 10
:()5-39-~--------Ben:0(b~Fluor~ntt1onc _________ : t I)
207-08-9--------Ben:oi·k)Fluorantt,ene _________ : I 0
50-3:-8---------Ben~o(a)Pyrene _______________ : 10
193-39-5--------Indeno(l,2,3-~d)Pyrene _______ : 10
53-70-3---------Diben~Ca,h)Anthracene ________ : 10
191-24-~--------Benzo(g,h,i)Perylene _________ : 10
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(1) -Cannot be separated from Diphenylamine 000696
FORM I SV-2 1/87 Re·
n
I 18
I
SEMIVDLAT!LE OFGAN!CS ANALYSIS DATA SHEET EPA SAMP:..£ NO.
X-F: l NSA ,::
I SAS N,:,.:
L.Jb S,ciinp 1 e ID: '30(16008:·:
I Sa.mole 1,,,1t/v,:,l: _1()00 (g/mL) ~ LE.1b F"'ile ID: 4 t..'060('8C:·-:
LG-vel: 0-3.t.e F:e,.:ei ved: ()6/('6/'3'(1
I % Moisture: not dee. de,:. Date E:·:traded: ()E,/(17 /"30
I E:,:t r .:i,: ti ,:,n:
IY/N' ~ pH:
1:.0tJT D-3.te Ana.l:1:ed:
Di 1 Ltt i ,:,n F" a,: t,:,r: 1. i) ~~---
I c,.:.,s nc.
(0/\J(ENTF'.•\ TI Or! !_l~J I TS:
( u,;: .'L ,: r ug ,'f·::9) ~~L.b_ Q
I 1 ,)8-·3::,-·.::--------Pt1 en,:, 1 ______________________ _
t11-44-4--------bi51_:-c1,1oroet ►1yl)Etf1er ______ :
~5-57-8---------~-1:f1l0r,~pt1cnol _______________ :
10 :u
10 :U
1 (I :u
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5·11-73-1---------1.3-Di~t,lor,:,ben:ene _________ _
11)6-46-7--------1,4-D1,:►1lorob~n:ene _________ _
101)-51-6--------Ben:yl Alcot,ol _______________ :
1 0 :u
1 (l :u
10 :u
95-51)-1---------1,:-Dt,:hloroben:eno __________ : 10 :u
I
95-48-7---------:-Mettiylphenol _______________ :
3~~38-3:-3------bi5<·:-1:t1lor,)is0pr,:,pyllEtf1er __ :
1,)6-44-5--------J-Mett,ylpt,enol ________________ :
10 :u
10 :u
1 0 :u
621-64-7--------tJ-rJitroso-Oi-n-Pr~pylamine ___ : 10 :u
I 67-7~-l---------He~acfilor,,ethane ____________ _
98-35-J---------Nitrobcn~ene ________________ _
78-59-1---------Isophorone ___________________ :
!O :u
ti) :u
10 :u
88-75-5---------:-Nitropf,enol ________________ : 10 :u
I 105-67-9--------2,4-Dimethylphenol ___________ :
65-85-0---------Ben:oic Acid ________________ _
1 0 :u
50 :u
111-91-1--------bis(:-Chloroetho•ylMethane ___ : 10 :u
I
120-83-2--------2, 4-0 i ,:h l or ,,pt,en,:,l ___________ :
120;,132-1--------1, 2, 4-Tr i ,:h 1 ,:-r,:,ben: ene _______ :
91-:-20-3---------N.aphthalen<> __________________ :
1 0 :u
10 :u
10 :u
106-47-8--------4-Chloroan1!1ne _____________ _ 10 :u
I 87-68-3---------Hexa,:hlorobutadiene _________ _
59-50-7---------4-Ct,loro-3-Mett,ylpt,enol ______ :
31-57-6---------2-Metf,ylnapf,thalene __________ :
10 :u
10 :u
10 :u
77-47-4---------Hexachlorocyclopentadiene ____ : 10 :u
I 88-01;-2------·---:2 ~ 4, 6-Tr i ,_: ti l ,_;ir ,:,ph ... :,n,:,l ________ :
~5-95-4---------2,4,5-Tri~hloropf1en0l ________ :
31-53-7---------2-Ct1l0r~napt1thalene __________ :
10 :u
50 :u
10 :u
I . .,.. "'·, .. 88-74-4---------~-N1troan1l1ne ______________ _
131-1!-3--------0imcthyl Phthalate ___________ :
:OB-96-8--------Acenaphthylene _______________ :
50 !U
10 :u
10 :u
606-20-2--------2,6-Dinitrotoluene ___________ : 10 :u
I FORM I sv-1 ------------------1/87 Re
000704
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!C Keystone DCI 061)c)8 -•)4-
SEMIVOLATILE ORGANICS ANALYSIS DAT.; SHEET
X-PJNSA-;:
Lab ,:,:,de: I EYTX Case N,:,. : 061)08
Lab Samp I e ID: ·c 1)1)f,1)08::•:
Sample 1,,Jt/,1,:,l: 1000 Lab Fi le ID: ➔LJ(,E,(J()SC:·;
Da.te Re,:eived: •)E,/()E,/"?(1
% MoistL1re: not dee. --/-
CONT
i::iF'C Cleanup:
(ScpF/C,:,nt/S0n~J
('(/N) b!..._ pH: 4.0 Dilution Fa~tor: :1~-~I) __ _
CAS NO. CJ:1F·OUND
CONCENTPAT!ON UNITS:
!ug/L or ug/Kg) UG/~
~9-•)9-:---------3-N1tr0Jn1l1n~------------·---s:-3:-3---------Acenaot,thene ________________ _
5 ! -·.:-3-5---------'2, 4-Di nit, r ,:,phen,:, l ____________ :
101)-c):-7--------4-Nitropt,enol ________________ :
132-64-9--------Diben:,~furan ________________ _
12!-14-:--------:.4-Dinitrotoluene __________ _
8J-66-:---------Di~tt,ylpf1th~latc _____________ :
7005-7:-3-------4-Ct1loropt1enyl-pf1enylether ___ :
8£-73-7---------FltJ•~renc ____________________ _
534-52-1--------4,6-Dinitro-2-Mett1ylpf1en0l ___ :
86-31)-6---------N-Nitrosodipt,enylamine (1) ___ :
11)1-55-3--------4-Bromopt1enyl-pt1enylot}1or ____ :
118-74-1--------Hexachloroben:ene ___________ _
87-86-5---------Pentacht,1rophenol ____________ :
95-01-8---------Phenantt,rene ________________ _
1~0-l~-7--------Anthracenc __________________ _
84-74-2---------Dl-n-8utylphthalate __________ :
:oG-44-0--------Fluaranthene ________________ _
129-:00-0-------Pyr ene ________________________ :
85-68-7---------Butylbencylphthalate _________ :
91 ~~-1---------3, 3' -Di ,:h l ,:,r ,:,ben:: i dine _______ :
56-55-3---------Ben:o<a)Ant•iracene __________ _
218-01-9--------Chrysene _____________________ :
117-81-7--------bis<:-Ethylhe,y!lPhthalate ___ :
117-84-0--------Di-n-Octyl Phthalate _________ :
105-99-2--------B~n:o<b)Flu,)r~nthen,1 ________ _
:07-08-3--------Ben:o(k)Fluorantt,ene ________ _
51)-32-8---------Ben:o(~)Pyrene _______________ :
193-39-5~-------Indeno(l,2,3-cd)Pyrene _______ :
53-70-3---------0ibenz(a,•1)Anthracene ________ :
191-24-2--------Ben:o(g,h,i)Perylene _________ :
Q
50 :u :o :u
51) :u
5(1 :u
I I) :u
10 :u
11) :u
10 :u
1( :u
5!) :u
S:) :u
10 :u
10 :u
10 :u
50 :u
1 (\ :u
10 :u
10 :u
10 :u
10 :u
10 :u
:o :u
10 :u
10 :u
I I
10 :u
11) :u
10 :u
10 :u
10 :u
1 I) :u
10 :u
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
------------------
000705
1/87 Re,
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18
SEMIVCLATILE OPGANICS ANALYSIS CATA SHEET _E;:·A SAMPL::: NO.
X-F: I NSA ~E
1 (l('lf) ( 9 I ml) tL_L __ Lab File ID: 4U06008( .:·1_:
Level : Date Pe,:eived: 1)6/1)7/~0
% Moisture: not de,:. dee. rate Extracted: 06,'09/90
pH: Dilution Factor: 1.0
C!JMF'OUND
CON(ENTF:APON IJMI TS:
(ug/L ,:,r u~/Kg) Ul;i/L
1('8-·?S-~--------Pf,enol ______________________ _
111-~4-4--------bis(::-ct,loroethyl)Ether ______ :
·:;15-5 7-8----.-----.:-1::h l ,:ir-,:,phen,:i l _______________ :
541-73-l--------1,3-Dict1lor,~ben:ene __________ :
106-46-7--------1,4-Di,:}1loroben:ene __________ :
l()(l-51-6--------Ben:yl Alcohol _______________ :
'35-50-1---------1,~-Di,:tiloroben:ene __________ :
95-48-7----------:-Methylpt,enol _______________ :
33638-3:-3------bis(~-Ct,l,)r•)is,,pr,)pyl)Ett,er __ :
106-44-5--------4-Methylphenol _______________ :
6~1-64-7--------N-Nitroso-Di-n-Pr,,pylamine ___ :
67-72-1---------He~achlor,)ethane ____________ _
98-95-3---------Nitroben:ene ________________ _
78-59-1---------Isophorone ___________________ :
88-75-5---------2-Nitrophenol ________________ :
105-67-9--------2,4-Dimethylpt,enol ___________ :
65-85-0---------Benzoic Acid ________________ _
!11-91-l--------bisl2-Ch!oroetho•ylMethane ___ :
120-83-2--------2, 4-Oi ,.:h 1 ,:ir,:iphen,::il ___________ :
120-8:-1--------1, 2, 4-Tr i ,: h I ,:ir,:,ben: ene _______ :
91-20-3---------Naphthalenff __________________ :
10G-47-8--------4-Chloroanil1ne _____________ _
87-68-3---------He,achlorobutadiene _________ _
59-50-7---------4-Chloro-3~Met,1ylp!1enol ______ :
91-57-6---------2-Methylnap,ithalene __________ :
77-47-4---------Hexachlorocyclopentadiene ____ :
88-O6-~----------2,4,6-Tric ►1l,Jrop ►1enol _______ _
~5-95-4---------:,•l,5-Trichloropt,enol _______ _
91-58-7---------2-(hlor•lnap~ith~lene _________ _
88-74-4---------:-N1troan1l1ne ______________ _
l31-t1-3--------01methyl Phth~lat~-----------
208-96-8--------Acenaphthylene ______________ _
606-20-:--------2,6-Dinitrotoluene __________ _
0
' ; ' 10 :u
10 :o
I 0 :u
10 :u
10 :u
10 :u
10 :u
I(, :u
I 0 :u
1 (l :u
1 (J :u
I 0 :u
10 :u
10 :u
1 (l :u
10 :u
51) :u
10 :u
10 :u
10 :u
10 :u
10 :u
10 :u
10 :u
10 :u
10 :u
10 :u
50 :u
10 :u·
50 :u
10 :u
10 :u
II) :u
----------------------------------------------------------------
FORM I SV-1 1/87
000717
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SEMI '/OU\ TI LE OF·::;:,r I l ,:s MIAL 'IS rs (),\ T ,\ SHEET
L~b rJame: ~-E'(STO~JE ENV,
SAS N,:,. : SDG N,:,. : (201...'..:.
1 ()(H)
de,:.
(YIN) N pH:
C.:..S NO. COMPOUND
corn
lab '3amp 1 e ID:
L.ab Fi le ID:
C Cl'~CENTF:,~ T ! OrJ UN I TS:
(ug/L or L1g/Kg) UG/L
3'?-,)·?-:----------3-Nitr,,dniline ______________ _
83-3~-g---------A,:enapt,tt,ene _________________ :
51-~8-5---------:,4-Dinitr,,pfion,,l ____________ :
1 (1()-(i:2-7--------4-N i tr ,:,phen,:,l ________________ :
13~-64-9--------Dibqn:ofur.Jn ________________ _
121-14-2--------~,4-Dinitrotoluene ___________ :
84-SG-~---------Oiett1ylpt,t~1alate _____________ :
7()05-7~-3-------4-Ct1loropt1enyl-pt1enylett1er ___ :
86-73-7---------Flu,)r~no _____________________ _
l0!)-10-£--------4-N1troan1l1ne ______________ _
534-~:-t--------4,6-Dinitr,,-:-Metf1ylp•1en,~l ___ :
86-31)-6---------N-NitrosodipJienylamin~ (!) ___ :
li)l-S5-3--------4-Bromopf1enyl-pf1enylether ____ :
118-74-1--------He~achlor,)ben=ene ___________ _
87-86-5---------Pentachlor,:,pfienol ____________ :
8~-,)1-8---------Pf,enanthrene ________________ _
120-12-7--------Anthra~ene __________________ _
84-74-2---------Di-n-Butylohthalate __________ :
:06-44-0--------Fluoranthene ________________ _
12'3,00-0--------Pyrene _______________________ :
85-68-7---------Butylbencylphthalate _________ :
91-94-1---------3, 3' -Di,: h 1 ,:ir ,:,benz i dine _______ !
56-55-3---------Benzo(a)Ant•ira,:ene __________ _
".::18-01-9--------Chrysene _____________________ :
117-81-7--------bis(2-Ethylhexyl)Phthalate ___ :
117-84-0--------Di-n-Octyl Phthalate _________ :
20~-·33-:--------Ben~o1b1Flu•~ranthene ________ _
:o7-()8-9--------BenzoC~:JFlu0rantf1ene ________ _
5()-3:-a---------Bcnzo(3)Pyrene _______________ :
193-39-5--------Indeno(l,2,3-cd)Pyrene _______ :
53-70-3---------0ibenzCa,h)Anthracene ________ :
191-24-2--------Benzo(g,h,i)Perylene _________ :
4UOE.Oc)SC ..:..::
0
51) :u
10 :u
50 :u
50 :u
10 :u
11) :u
1 (, :u
1 (J :u
t i) :u
so :u
Sc) :u
10 :u
1 t) :u
11) :u
50 :u
10 :u
10 :u
10 :u
10 :u
10 :u
10 :u
~c) :u
10 :u
10 :u ,, :J
10 :u
1 ,) :u
10 :u
11) :u
10 :u
10 :u
10 :u
-------------Ill -Cannot be separated from Diphenylamine 000718
FORM I SV-2 1 /87 Re,
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PESTICIDE ORGANICS ANALYSIS DATA SHEET
Lau Code: f. EiTX SAS No.: SDG No. : C2<:•WA
Matr1;<: (soil/water) WATER Lab Sample ID: 9(11)68-022A
Sample ..,t/vo\: 1 l)t)(J <g/ml) ML Lab File ID:
Leve t : LOW Date Received: 1)6/1)6/~0
¼ Moisture: not dee. dee. Date Extracted: 06/09/90
E.":traction: CSepF/Cont/Sonci CONT Date Ana\y:ed: 06/22/90
GPC Cleanup: (Y;N) N pH: 7.0 Dilution Factor: 1.00
CAS NO. COMFOUNC•
CONCENTRATION UNITS:
lug/Lor ug/Kgl UG/L
319-24-6--------alpha-BHC ___________ _
319-85-7--------beta-BHC ___________ _
31·~-8~.-8--------delta-8HC ___________ _
58-83-·~---------g~rnma-BHC CL1ndanel _____ _
76-44-8---------Heptachlor __________ _
30~-()0-2--------Aldrin ____________ _
1 i.J24-:",7-~-------Heo t ach l ,~1-eoa:·: 1 de _____ _
~59-~8-8--------EnooEulfan ! __________ _
6(,-57-1---------Dieldi-in ___________ _
72-55-·~---------q,4'-DD~------------72-21)-8---------Endrin ____________ _
33213-65--~------Endasulfan II ________ _
72-54-8---------4,4'-DDD __________ _
1031-07-8-------Endosulfan sulfate _____ _
51)-29~3---------4,4 1 -DDT ___________ _
72-43-5---------Methoxychlor _________ _
53494-70-5------Endrin ketone ________ _
5108-71-9-------alpha-Chlordane _______ _
5103-74-2-------gamma-Ch\ordane _______ _
8001-35..:Z-------Toxaphene_...,... _________ _
12b74-1i-2------Aroclor-1016 ________ _
11104-28-2------Aroc\or-1221 ________ _
11141-lb-5------Aroclor-1282 _________ _
534b9-21-9------Aroc\or-1242 _________ _
12672-29-6------Aroclor-1248 ________ _
11097-69-1------Aroclor-1254 _________ _
11096-82-5------Aroclor-1260 _________ _
FORM I PEST
0 .05(, :u
c,.o~~o:u
1) .1)51) :u
(1 .(,50 :u
(1.(151) :u
(i .050 :u
1) • \):,,) : u
!) .(151) :u
0.1(1 :u
(,.1(,:u
0.10:u
0. 10 :u
0. 10 :u
0.10:u
0. 10 :u
0.51) :u
0. 10 :u o.so:u o.so:u
1 .o :u o.so:u o.so:u o.so:u
o.5o:u
0 .5•) :u
1 .0 lU
1 .t) :u
Q
001393
1/87 Rev.
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ID EPA SAMF·LE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
Lab Name: ~EYSTONE ENV.
Lab Code: 1•.E'/TX Case No. : l)!;.(H)8 SAS No.: SC1G No . : C30WA
Mat,-i: : <s.::n \/water) WATER Lab Sample ID: 901)68-()25A
Sample wt/vol: (g/mL) ML Lab Fi le ID:
Level : ( 101./med) LOW Date Received:
¼ Moisture: not dee. dee. Date E;dracted:
<SepF/Cont/Sonci
1'1/N) N
CONT Date Analy:ed: 0~/23/90
GPC Cleanup: pH: Dilution Facto1·: 1.00
COMf-·OUNC•
CONCENTRATION UNITS:
(ug/L or ug1Kg1 UG/L
819-84-~--------alpha-BHC ___________ _
31~-85-7--------beta-BHC ___________ _
31~-8~-s--------delta-BHC __________ _
58-8·~--~---------gamma-BHC (Lindane) _____ _
7~-44-8---------Heptachlor __________ _
31:19-t)0-2--------Aldrin ____________ _
1024-57-3-------Heptachlor epo~<ide _____ _
359-33-S--------Endosulfan ! _________ _
E,,)-57-1---------Dieldrin ------------72 -55 -~ - - - - - - - - -4, 4 ' -DD E ___________ _
72-20-8---------Endrin ____________ _
33213-65-·~------Endosulfan II ________ _
72-54-8---------4,4'-DDD ___________ _
1031-07-8-------Endosu\fan sulfate _____ _
50-29-3---------4 ,4 '-DDT ___________ _
72-48-5---------Methoxych\or _________ _
534'34-70-:5------Endr in ketone ________ _
5103-71-9-------•lpha-Ch\ordane _______ _
5103-74~2-------gamma-Ch\ordane _______ _
8<)01-354!-------Tox•phene __________ _
12E. 74-11--2------Aroc \or-1 <) 1 '=> _________ _
11104-28-2------Aroc\or-1221 ________ _
11141-16-5------Aroc\or-1232 ________ _
534E.9-21-9------Aroc\or-1242 _________ _
121:>72-29-b------Aroclor-1248 _________ _
11097-E,·3-l------Aroc \or-1254 _________ _
110'36-82-5------A1·oc \or-12b0 _________ _
FORM I PEST
t) .55: X
1) .050 :u
o.oso:u
0.064!X o.,w :x
I) .051) :u
o.oso:u
0.1)50:U
o.as:x
() .10 :u
0.10:u
0.7b:X
0 .10 :u
0. 10 :u
o.s·;-:x
0.50:U
0.10:u
I) .51) :u
o.~o:u
1 .o :u
0.50:U o.so:u
0.50:U o.s,,:u
f) .50 :u
1 .o :u
1.0:u
Q
001398
1/87 Rev,
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PESTICIDE ORGANICS ANALYSIS DATA SHEET EF·A SAMPLE NO .
Lab N•me: KEYSTONE ENV. Contract: 17·~281)-0~
S-10-FB(0-2)
Lab Code: ,:EYTX Case No.: O'::,(H)8 SAS No.: SDG No. : C30WA
Lab Sample ID: ~0068-007A
Lab Fi le ID:
(s01l1wa\eri SOIL
Sa.mp le wt/ vo 1 : 30 .0 (g/mU G
Level : (low/medi LOW
X Moisture: not dee. 34 dee.
E·<tr-act 10n: <SepF/Cont/Sonc> SONC
GFC Cleanup: iY/N) N pH: 5.4
Date Received: 1)6/02/90
Date Extracted: 0~/06/90
Date Analyzed: 06/22/90
Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
<ug/L or ug/Kgl UG/KG
31'3-84-6--------alpha-BHC -----------31~-85-7--------beta-BHC ___________ _ 12
12
313-86-8--------delta-8HC __________ _ 12
53-89-3---------gamma-BHC (Lindane) _____ _ 12
76-44-8---------Heptachlor __________ _ 12 3()'~-00-2--------Aldrin ____________ _ 12
11:124-57-3-------Heptachlor epox1de _____ _ 12
95·3-98-8--------Endosulfan I 12
60-57-1---------Dieldrin __________ _ 2'1 72-55-~---------4,4'-DDE ___________ _ 24
72-21)-8---------Endrin ___ ~---------
33213-~5-~------Endosulfan II ________ _
24
24 72-54-8---------4,4'-DDD ___________ _ 24
1031-07-8-------Endosulfan sulfate _____ _ 24
:u :u
:u
:u
:u :u
:u :u
:u :u :u :u :u :u 50-29-3---------4,4'-DDT ___________ _ 0.6,) :JX
72-43-5---------Methoxychlor _________ _ 120 :u 53494-70-5------Endrin ketone ________ _ 24 :u
5103-71-9-------alpha-Chlordane ______ ...,....
5103-74-e-------gamma-Chlordane _______ _
120 :u
120 :u
S001-35-2-------Toxaphene __________ _ 240 :u
12b74-11-2------Aroclor-10lb ________ _ 120 :u
11104-28-2------Aroclor-1221 ________ _ 120 :u
11141-16-5------Aroclor-1232 ________ _ 120 :u
53469-21-9------Aroclor-1242 _________ _ 120 :u
12672-29-b------Aroclor-1248 _________ _ 120 :u
I 10'37-69-1------Aroc lor-1254 _________ _ 240 :u
I I 0'36-82-5------Aroc l or-1260 _________ _ 240 :u
FORM I PEST
a
001403
1/87 Rev,
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ID EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
S-1 <)-FB ( 2-4 >
Lab Name: KEYSTONE ENV. Contract: 17~280-1)4
Lab Code: I: EYTX Case No. : ()f:.(1(18 SAS No.: SDG No. : C30WA
Matri:<:: (soil/water) SOIL Lab Samp t e ID: ':l(H)f:,8-(i l l)A
Sample wt/vol: 30.0 (g/mLl G Lab Fi le ID:
Level : (\ow/med) LOW
¼ MoistL1re: not dee. 22 dee.
Date Received: 06/1)2/90
Date E~tracted: 06/06/90
E>::traction: t SepF /Cont /Sane)
tY/NJ N
SONC
pH: 4. 8
Date Analyced: OS/22/90
GFC Cleanup: [11 lut ion Fiictor:
c.:.s NO. COMF'OUNC<
CONCENTRATION UNITS:
(uq/L or ug/Kg> UG/KG
:31 :1-84-1:,--------a lpha-DHC ___________ _
313-85-7-~------beta-BHC ___________ _
31·~-86-a--------delta-8HC ___________ _
58-S·~-·~---------gamma-8HC (L1ndane~------
10
1(1
10
I<)
1 .(n:..,
Q
:u :u :u :u
7S-44-8---------Heptachlor __________ _ <).12 :.ix
309-00-2--------Aldrin, ____________ _ I 0 :u
11)24-57-3-------Heptachlor epoxide _____ _ l (l :u
~59-98-8--------Endosulfan I _________ _ 10 :u 60-57-1---------Dieldrin, ___________ _ 21 :u 72-55-9---------4,4'-DDE ___________ _ 21 :u 72-20-S---------Endrin, ____________ _ 21 :u
33213-~5-i------Endosulfan II ________ _ 21 :u 72-54-8---------4,4'-D00 ___________ _ 21 :u
1031-07-8-------Endosulfan sulfate _____ _ 21 :u 5 1)-29-3---------4,4'-DDT ___________ _ 21 :u
72-43-5---------Mathoxychlor _________ _ 100 :u
53494-70-5------Endrin ketone ________ _ 21 :u
5103-71-~-------•lpha-Chlordane _______ _ 100 :u
5103-74-2-------gamma-Chlordane _______ _
8<)01-35-2-------Toxaphene ___________ _
100 :u
210 :u
12674-11-2------Aroc lor-1016 ________ _ 100 :u
11104-28-2---.---Aroclor-1221 ________ _ 100 :u
11141-16-5------Aroclor-1232 _________ _ 10•) :u
5346•:i-2 I -9'------Aroc \ or-1242 _________ _ 100 :u
126 72-2':i-6------Aroc lor-1243 _________ _ 100 :u
110~7-69-1------Aroclor-1254 _________ _ 210 :u
11 O~t,-82-5------Aroc 1 or-1261) _________ _ 210 :u
---
001408
FORM I PEST 1/87 Rev.
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ID EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
S-10-FBC2-4>
Lao Name: KEYSTONE ENV.
Lab Code: VEYTX Case No. : ()t,(J1)8 SAS No.: SDG No. : C30WA
Lab Sample I [I : •;i(u)'::,8-(, 11 A
S"mp\e wt/vol: 30.0 Cg/mL) G Lab Fi I e ID:
Leve I : Clow/med) LOW
1/. Moisture: not dee. 22 dee.
Crate Received: (H:./(12/•:f(l
Date E::::t r acted: 06/(1f:,;·:-10
Date Ana\y:ed: 06122/30 £,..,traction: CSepF/Cont/Sonci SONC
GF·C CI eanup: (Y/N) N pH: '1.7 01 lut ion Factor: 1.<)0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg> UG/kG
319-84-6--------alpha-BHC __________ _ 10
319-85-7--------beta-BHC ___________ _ 10
319-86-8--------delta-BHC __________ _ 10
58-8~-9---------gamma-BHC (l1ndane) _____ _ 10 76-44-8---------Heptach\or __________ _ 10
309-01)-2--------Aldrin ____________ _ 10
102q-57-3-------Heptach\or epoxide _____ _ 1 (1
·;15·1-·:18-8--------Endosu 1 fan I _________ _ 10
~-0-57-1---------Dieldrin ___________ _ 21
72-55-~---------4,4'-DDE ___________ _ 21
72-20-8---------Endrln ____________ _ 21
33213-65-~------Endosulfan II ________ _ 21 72-54-8---------4,4'-DOO ___________ _ 21
1031-07-8-------Endosulfan suliate _____ _ 21
50-29-3---------4,4'-DDT ___________ _ 21
72-48-5---------Met ho:-:yc:h l or _________ _ I <)0
53'194-70-5------Endrin ketone ________ _ 21
5103-71-9-------•lpha-Ch\ordane _______ _ 100
5103-74~e-------g.mm•-Chlordane _______ _ 100
8001-35-2-------Toxaphene __________ _ 210
12674-11~2------Aroclor-1016 _________ _ 100
11104-28-2------Aroc:\or-1221 ________ _ 100
11141-16-~------Aroc\or-1232 ________ _ 100
5346·~-21 -9------Aroc I or-1242 _________ _ 100
12672-29-6------Aroclor-1248 ________ _ 100
11097-69-1------Aroc:\or-1254 _________ _ 210
11096-82-5------Aroc 1 or-12b0 _________ _ 210
FORM I PEST
Q
:u
:u
:u :u :u :u
:u
:u
:u
:u :u
:u :u :u :u
:u
:u :u :u
:u :u :u :u :u :u
:u :u
---
001413
1/87 F.ev.
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ic,
PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: kEYSTONE ENV. 5-l 3A-FB ( <)-2
Lab Code: fiE\'TX SAS No.: SDG No. : C3OWA
Mat.ri>:: (s01 I/water) SOIL Lab Samp 1 e ID: °:f(H)f:.8-(, 12A
Samp 1 e w t/vo I : 3() .0 <glmll G Lab Fi le ID:
Level: Clow/med) LOW
¼ Moisture: not dee. 23 dee.
Date Received: Of:,/02/90
Date Extracted: 06/06/90
Date Analyzed: 06/22190 CSepF/Cont/Soncl SONC
GF·C CI eanc1p : CY/Nl N pH: 4.7 Dilution Factor: 1.00
c~s NO. COMPOUN[1
CONCENTRATION UNITS:
(ugiL or ug/Kgl UG/KG
313-84-6--------alpha-BHC ___________ _
31~-85-7--------beta-BHC ___________ _
319-86-2--------delta-8HC~~---~-----
58-8S-~---------gamma-BHC (Lindane~------
76-~4-8---------Heptachlor __________ _
309-(10-2--------Aldrin~------------
1(124-57-3-------Heptachlor eoo~<ide ____ _
35·~-38-8--------Endosulfan ! _________ _
~0-57-1---------0ieldrin ___________ _
72-55-9---------4,4'-DDE ___________ _
72-20-S---------Endrin~-~=---------
33213-~5-3------Endosulfan II ________ _
72-54-8---------4,4'-DDD __________ _
1031-07-8-------Endosulfan sulfate _____ _
5,)-29-3---------4 ,4 '-DDT...., __________ _
72-43-5---------Methoxych\or _________ _
53494-70-~------Endrin ketone ________ _
5103-71-9-------•lph•-Ch\ordane _______ _
5103-74-E-------gamma-Chlordane _______ _
81)1) 1-35-1?-------T oxaphene.,.... __________ _
12674-11~2------Aroc\or-1016 ________ _
11104-28-2------Aroclor-1221 ________ _
11141-16-5------Aroclor-1232 ________ _
53'1€,3-21-"3------Aroc \or-1242 _________ _
12672-29-6------Aroclor-1248 ________ _
11097-69-1------Aroc\or-1254 _________ _
11091::,-82-5------Aroc 1 or-1260 _________ _
FORl'I I PEST
11)
1 (l
10
10
10
11)
10
l <)
21
21
21
21
21
21
21
10<)
21
100
100
210
100
100
100
100
100
210
210
Q
:u
:u
:u
:u
:u :u :u :u :u
:u
:u :u
:u :u :u :u :u :u :u
:u
:u :u
:u
:u :u
:u :u
---
001418
1/87 Rev.
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ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET EF'A SAMPLE NO .
Lab Name: KEYSTONE ENV. Contract: 17~280-i)4
S-13A-Fll(2-4
L.;o Code: f.EYTX Case No. : (JE,(11)8 SAS No. : SDG No. : C3<:•WA
Matri:,,:: <soi \iwateri SOIL
Sample wt/vol: 30.0 (g/mU G LabF1\eID:
Leve\ : (\o.,./med) LOW
¼ Moisture: not dee. 22 dee.
Date Received: 06/(12/90
Date Extracted: 0~/06/·~1)
Date Analv:ed: 06/22/9(1 E~-:t1-act ion: (SepF/Cont/Sonc) SONC
GF·C C\eanc,p: (Y/N) N pH: 4.7 Dilution Factor: I .O<)
CAS NO. COMFOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg> UG/~G Q
319-84-6--------a\pha-llHC ___________ _ 3.o:Jx 21 ':1-85-7--------bet a-BHC ___________ _
31 ·:f-SE,-8--------de l t l:\-BHC ___________ _
58-89-9---------gamma-BHC
76-44-8---------Hep~achlor
(lindane)
309-00-2--------Atdrin ____________ _
1024-57-3-------Heptachlcr
·:159-98-8--------Endosulfan
epox1de
I
60-57-1---------Dieldrin ___________ _
72-55-9---------4,4'-DOE ___________ _
72-20-8---------Endrin ____________ _
33213-65-9------Endosulfan II ________ _
72-54-8---------4,4'-DDD ___________ _
1(131-07-8-------Endosulf an su \ fate _____ _
50-29-3---------4,4'-DDT ___________ _
72-43-5---------Methoxych\or _________ _
53494-70-5------Enctrin ketone ________ _
5103-71-9-------a\pha-Chlordane _______ _
51<)3-711-2-------gamma-Ch\ordane _______ _
8001-35'-e-------Toxaphene
12674-11-2------Aroc\or-1016 ________ _
11104-28~2------Aroc\or-1221 _________ _
11141-16-5------Aroc\or-1232 ________ _
5346':1-21-9------Aroc \ or-1242 _________ _
12672-29-6------Aroc\or-1248 ________ _
110·,n-6·:1-1------Aroc \or-1254 _________ _
111)·~6-82-5------Aroc \or-1260 _________ _
FORM I PEST
13 :x
lt) :u
10 :u
1 (I :u
10 :u
1 (J :u
1 0 :u
21 :u
21 :u
21 :u
14 :JX
21 :u
21 :u
1.s:Jx
18 : JX
21 :u
100 :u
I .6: JX
210 :u
100 :u
100 :u
100 :u
100 :u
100 :u
210 :u
210 :u
001423
1/87 Rev.
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I [I EF·A SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
S-I 3A-FE< ( 2-4) :
Lci.b r·J,;,ne: fc'EYS fONE ENV.
Lao Cude: f-EYTX Case No • : 1)f:,c)i)8 SAS No.: SDG No. : C30WA
Matri.,.,;: (soi l/wate1-J SOIL
Sample wt/vol: 30.0 <glmL> G Lab File ID:
Level : ( I ow/med) LOW Date Received: 0~/(,2/90
1/. Moisture: not dee. 20 dee. Date Extracted: 06/06/90
<SepF/Cont/Sonc) SONC Date Analyzed: 06/22/90
GF·C C \ eanup: (Y/N) N pH: 5.1 Dilution Factor: 1 .00
CAS NO. COMPOUND
CONCENTF:ATION UNITS:
lug/Lor ugtKgl UG/KG
319-84-6--------aloha-BHC ___________ _
31 ·:!-85-7--------bet a-BHC ___________ _
31·;-86-8--------delta-BHC ___________ _
58-8~-9---------gamma-BHC <L1ndane> _____ _
7~-44-8---------Heptachlar __________ _
30'3-t)t)-2--------A l dr in ____________ _
11)24-57-3-------Heptachlo~ eoo~1de _____ _
95'3-~8-8--------Endosulfan I _________ _
60-57-1---------Dieldrin ___________ _
72-55-':1---------4 • 4 '-DOE ___________ _
72-20-8---------Endrin ____________ _
33218-65-9------Endosulfan 11 ________ _
72-54-8---------4,4'-0DD ___________ _
1031-07-8-------Endosu I fan su I fate _____ _
50-29-3---------4,4'-DDT ___________ _
72-43-5---------Methoxychlor _________ _
53494-70-5------Endrin·ketone ________ _
5103-71-9-------alpha-Chlordane _______ _
5103-74-2-------gamma-Chlordane _______ _
8001-35...:e-------Toxaphene __________ _
12674-11~2------Aroclor-1016 ________ _
11104-28-2------Aroc\or-1221 ________ _
11141-16-5------Aroclor-1232 ________ _
53469-21-9------Aroclor-1242 _________ _
12672-29-6------Aroc\or-1248 ________ _
I 10'37-6'3-1------Aroc I or-1254 _________ _
11096-82-5------Aroc l or-1260 _________ _
10 :u
10 :u
1,) :u
1(, :u
ti) :u
10 :u
10 :u
1 t) : U
4 .':. ! J X
20 :u
2<) :u
20 :u
20 :u
20 :u
0.12:Jx
18 : JX
20 IU
100 :u
100 :u
2<)0 :u
100 :u
100 :u
100 :u
100 :u
100 :u
200 :u
200 :u
Q
i ..
001428
FORM I PEST 1/87 Rev.
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'JOLATILE OF:GMJICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
fC:eyst one DC11 06008 -,H-
EPA SAMPLE NO.
Case N,:,. : OE.008
Sample "'t /v,,1: 5.0 (g/mU i:!b_
Level : (l,:,1,,1/med) LOW
% Moisture: not dee.
PACK
rlumber TI Cs f ,:,und: __
CAS NUMBEf;• COMPOUND NAME
C-3C'-WA
SAS No,: 5Dr3 Ne,. : C30WA
Lab S--1mo le ID:
Lab File ID:
Date Pe,:~ i '/="d:
Date Analysed:
Diluti,)n Fa,:tor:
CONCENTPAT ION UN ITS:
(ug/L ,:,r ug/kg) U(5/L
'300600802
5U06008V(\:A
06/<) l /"31}
OE./05/'30
1.0
F:T EST. CONC •.
000041
FORM I VOA-TIC 1/87 Rev
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• IE
VOLATILE OR•,AN!CS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Keystone OCI 06008 -o4-
_EPA SAMPLE NC
C-!5!5A
L3b Name: ~EYSTONE ENV. C,:,ntra,:t: 17'3'280-04
Lab C,:,de: f,EYTX Case No:i.: 06003 s~s No.: ----SDG No.: C30WA
Matrix: (s,oil /•Jater) WATEF:
Sample wt/vol: 5.0
Level: ( I ,,w/med) LOW
% Moisture: not dee.
C,:il umn (pa,:k/,:ap) PACK
NLtmber TIC-s f1:,und: _Q
CAS NUMBER
(g/ml) !'.!k...._
COMPOUND NAME
Lab Samp I e ID: '300600804
Lab File JO: 5U06008V04
Date Received: 06/01/'30
Date Analy:ed: 06/04/'30
Dilution Factor: &1~--0 __ _
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC; Q
----------------------------------------------------
FORM I VOA-TIC 1/87 RE
000050
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• lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Keystone OCI 06008 --04-
EPA SAMPLE IJO.
L3b ~lame: f EYSTONE ENI/.
Lab C,:,de: t.E'{TX ("3se No.: 06008
M.Jtri:-': (s,:,il/\Jater) l.JATEP
Sample 1,1t /v,:,J: 5.0 (g/mL) t'.!L_
Level: LOW
% Moisture: not dee.
C,:,l umn fpa,: k/,::.ap) PAO'.
Number TICs f,:iund: _Q
CAS NUMBER COMPOUND NAME
SAS N,:,.:
C-90A
SDl3 No.: C30WA
L3b Sample IO: 9006008::
Lab File IO: 6U0600SV::
Date Received: 06/07/90
Date Analyzed: 06/14/90
Dilution Factor: 1.0 ~~--
CONCENTRATION UNITS:
(ug/L ,:,r ug/Kg) IJ§LL
RT EST. CONC; Q
' ' '--------------------------------------------·-------------------------
FORM I VOA-TIC I /87 Re
000084
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IE
VOLATILE OR'3Ml: CS ANAL YS I 5 DAT A SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Keystone DC• 06008 ~4-
_EPA SAMPLE: NO.
C-'::IIA
Lab Name: KEYSTONE ENV. Contract: 179280-()4
Lab C,:,de: KEYTX Case N,::..: l)E,008 SAS No.: ____ so,, No.: C30WA
Matrix: (scil/waterl WATER
Sample wt /v,ol: 5.0
( 1 ow/med) LOW
% Moisture: not dee.
(pack/capl PACK
Number TICs fo:iund: ~
CAS NUMBER
(g/mLl ~
COMPOUND NAME
L<1b Sample ID: '?OOE.00825
Lab Fi le ID: 4U06008V:5
Date Received: l)E,/07 /'30
Date Analyzed: 06/15/'30
Di I ut i ,,n Fact ,,r : :.1..,_.-"0'---
C:ONCENTRA T ION UN ITS:
(ug/L ,,r ug/Kg' UG/L
.: :
RT EST. CONC. : C!
FORH I VOA-TIC 1/87 Re,
000091
I
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• IE
VOLATILE OF:I',AN I CS ANALYSIS DA TA SHEET
TENT A Tl '.'ELY I DENT IF I ED COMPOUNDS
Key.-tone DCI 06008 -04-
_EPA SAMPLE NO.
Lab Name: KEYSTONE EN'/.
Lab C,:,de: VEYTX Case N,:i.: 06008
M.3.tri:<: (soil/water) WA TEP
Sample wt /v,)l : 5.0 (g/mU t!b_
Level: ( 1 ,:,w/med) LOW
'1/. MoistuYe: n,:-,t dee.
1:,:,l umn (pa,:k/,:ap) PACK
Number T!Cs f,:,,,nd:
S-RINSATE
SAS N,:,.: SDG No. : C30WA
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTF:A Tl ON UN ITS:
(ug/L or ug/Kg) UG/L
900600815
5U06008VIS
06/02/90
06/04/90
1.0
, ' . '
CAS NUMBEF: COMPOUND NAME F:T EST. CONC{ : g
'. ===~-: : . . : T: :
' I I I o I ----------------------------------------------------------------------
000127
FORM I VOA-TIC 1 /87 Re,
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• IE
VOLATILE OF:GANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Keygtone OCI 06008 --04-
_EPA SAMPLE NO.
TRIPBLANt'.
L•b Name: KEYSTONE ENV. C,:,n tr a,: t : I 7·3:::80 ,)4
Lab Cc,de: KEYT X Case Ni:i.: l)E,008 SAS N,:,. : ____ 5013 No. : C30WA
Mat r i " : ( s,:, i I /water ) WA TEP
Sample wt/vol: 5.0
Level: LOW
% Moisture: not dee.
Column (pa,:k/cap) PACK
Number TICs found: __ I
CAS NUMBER
Cg/mU t!!:.__
COMPOUND NAME
Lab Sample 10: 90(1600821
Lab Fi le IO: 4UOE,008V:1
OE,/OE,/90
Date Analyzed: 06/09/90
Oiluti,on Fact,,r: 1.0 ~-"'---
CONCENTRATION UN ITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC.· g
:=-==========~===:---·====---------------------:---=-=--:---==========:---==:
!. 7446-09-5 :SULFUR OIOXIDE(ACN)(OOTl 1. 10 : 1500 · : J
' ' ·--------------------------------------------·--------
FORl'I I VOA-TIC 1/87 Re•
000138
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•
...... --.....
IE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Key .. tone DCI 06008 -04-
_EPA SAMPLE NO
TRIPBLANY
L~b Name: KEYSTONE ENV, Contract: 179280-04
Lab C,:,de: KEYTX Case No.: 06008 SAS No.: ____ SDG No.: C30WA
Matri•: (soil/water) WATER
Sample wt/vol: 5.0 (g/mU !1b_
Level: LOW
'l. Moisture: not dee.
C,:,l umn PACK
Numbt?r TIC·3 found: ____Q
CAS NUMBER COMPOUND NAME
Lab Sample ID: '300600806
Lab File ID: 5U06008V06A
Date Pe,:eived: 06/01/'30
Date Analy=ed: 06/05/90
Di 1 ut ion r c1ct•:-ir: ~1~•~0 __ _
CONCENTRATION UN ITS:
(ug/L o:,r ug/Kgl UG/L
RT EST. CONC~-Q
----------------------------------------------------------------------
FORM I VOA-TIC 1/87 Re
000146
I
I •
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I;
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I
I ..... ~-"'.
I
. ( i. -.
I
...
IE
VOLATILE OR1~ANICS ANALYSIS DATA SHEET
TENTATIVELY IDENT!f!ED COMPOUNDS
Keystone DCI 06008 -04-
EPA SAMPLE NO.
TR I PBLANI<
L3b Name: KEYSTONE ENV. Contract: 179:80-04
Lab C,~de: KEYTX Case No.: 06008
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/ml) t!L_
Level: (!ow/med) L~O~We,__
r::,:,l umn (pa,: k /,: ap) PACK
tJumber TICs found: _Q
CAS NUMBER COMPOUND NAME
SAS No. : SDG No.: C30WA
Lab Sample ID: 9(~600817
Lab file ID: 5UOE.0081/!?
Date Re,:ei ved: 06/02/'30
Date Analy:ed: 06/05/'30
Oiluti,,n F"a,:f;.:,r: 1.0 ~-"----
CONCENTRATION UNITS:
lug/L or ug/kgl UG/L
PT EST. CONC~ Q
----------------------------------------------------------------------
•
fORM I VOA-TIC 1/87 Re•
000156
I
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I
I
I
IE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Keystone DCI 06008 --04-
_EPA SAMPLE NO.
X-RINSATE
Lab Name: KEYSTONE ENV. Contract: 179280-c)4
Lab C,:,de: KEYT X Case N,:,.: 061)08
Matrix: (soil/waterl WATEP
Sample 1o1t/vc,I: 5.0 (g/mL) t1b..._
Level: ( l ,~,.,/med) L=O=W~-
X Moisture: not dee.
C,:,l umn (pack/,:ap) PACK
Number TICs found: __ 1
CAS NUMBER COMPOUND NAME
SAS N,,.: ____ SDG No.: C30WA
Lab Sample ID: 301)61)08:cl)
Lab Fi le ID: 4U06000v:::o
Date Received: 06/06/30
Date Analy=ed: 06/03/30
Di I ut i ,,n Fa,:tor: I. O =~--
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC. Q
:==-===-=~=-===-=:----------------------------:--------:-----=---==~=:-----:.
1. 7446-03-5 :SULFUR DIOXIDE(ACN) (DOT) 1. 35 : I 10 : J
I t I I
----------------·----------------------------·--------·-------------'
f"ORM I VOA-TIC 1/87 Re,
000163
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I·
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I
I
I
I
I
IE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Kay11tona DCI 06008 ->4-
_EPA SAMPLE NO.
X-RINSATE
Lab Name: KEYSTONE ENV. C,:,n tr ..3C t: 1 79280-1)4
Lab 1:0:,de: KEY TX Case N,~.: 06008 SAS No. : SDG No.: C30WA
Matri:c (:.,:,ii/water) WATER
Sample .it/v,:,l: 5.0
Level: ( t ,:iw/med) LOW
'l. Moisture: not dee.
C1:il umn (pa,: k / ,: ap) PACK
Number TICs found: __ I
CAS NUMBER
1. :UNKNOWN
(g/mU t'.!.b__
COMPOUND NAME
Lab Sdmp 1 e ID: 900600826
Lab File ID: 4U06008V26
Date Received: 06/071':!0
Date Analyzed: 06/15/90
Dilution Factor:~!~·~•) __ _
CONCENTRATION UNITS:
<ug/L or ug/Kg) UG/L
RT EST. CONC.~
I. 60 :
g
FORM I VOA-TIC 1/87 Re•
000173
I
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I
• IE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Keyst<Jne DCI 06008 -¢4-
_EPA SAMPLE NO.
X-RINSATE
Lab Name: KEYSTONE ENV, C,,n tract: I 7·3:280-<)4
Lab ,:,,de: l<EYTX 06008 SAS No,: ____ SDG No.: C30WA
M~trix: (soil/watar) WATER Lab Sample ID: 900600816
Sample wt/v<Jl: 5.0 (g/mL) !:!h___ Lab File ID: 5U06008Vl6
Level: <low/med) LOW
: M<Jisture: not dee,
(pa,:k/cap) PACK
Number TICs f,:iund: __Q
CAS NUMBER COMPOUND NAME
Date Re,:eived:
Date Analyzed: 06/05/90
Dilution Factor: ~l~·~0 __ _
CONCENTRATION UNITS:
(ug/L or ug/Kg) lJ§.L1__
RT EST, CONC,: 0
----------------------------------------------------------------------
FORM I VOA-TIC 1/87 Re
000183
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• IE
VOLATILE OP13AN!CS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Key~tone DC• 06008 --04-
_EPA SAMPLE NO.
KOPPERS
L.>b Nume: f:EYSTONE ENV. C,:,nt r .>•: t:: I 7"3280-04
Lab Code: KEYTX Case No.: OE.008 SAS N,,.: ____ SDG No.: C30WA
Matrix: !soil/water) SOIL
Sample wt/vol: 5.0
Level: ( 1 ,:,w/med) LOW
% Moisture: not dee. ___u
Column lpack/,:ap)
Number TICs found: __ I
(g/mU §_
Lab Sample ID: 900600830
Lab Fi 1 e IO: 4U06008V30
Date Re,:ei ved: OE,/01/90
Date Analyzed: 06/12/90
Oiluti,:,n F'act1:ir: 1.0 ~~---
CONCENTRATION UNITS:
lug/Lor ug/Kgl UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONG.; Q
:---==-=========-:==---==----=----------------:--------l--========= ~:=====:
I, :UNKNOWN 1. 70 : lS ~ lJ
' ' '----------------'------------------------------------------------------
FORM I VOA-TIC 1/87 Re,
000188
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•-IC.
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IE
VOLATILE OPGANICS ANALYSIS DATA SHEET
TENTATIVELY I DEN TI FI ED COMPOUNDS
Keystone DCI 060<)8 --04-
_EPA SAMPLE NO.
S-10-FB<O-.::) Lab Name: KEYSTONE ENV. C,:,n tr -1,: t: l 7'3280-()4
Lab Code: KEYTX Case No.: 06008
Ma.tr i .'(: (3,:,i l/w1ater) SOIL
Sample wt /v,:il: 5.0 (g/mU §__
Level: ( l 1:iw/med) LOW
% Moistt1re: not dee. 34
1::,,1 umn (pa,:k/,:ap) PACK
Number TICs found:
CAS NUMBER COMPOUND NAME
SAS No.: SDG No.: C30WA
L.1b S-ample ID:
Lab File ID:
Date Received:
Date Analyzed:
Di Jut ion r.a,:tor:
CONCENTRATION UNITS:
<ug/L ,,r ug/Kg) UG/KG
900600807
4U06008V07
1)6/02/"?0
06/08/90
1.0
. ' -= ' RT EST. CONCi. : g : ================: -:;:;:;.,.;: ______________________ , ___ : -==-----: ====-======~ ! ----=:
I. 744€.-0"3-5 :suLFUF: DIOXIDE(ACNJ<DOTl 1.50: 730! :J
-. : UNKNOWN 4. 90 : 23 : J
' '----------------------------------------------------------------------
FORM I VOA-TIC 1/87 Re,
000200
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l I --
1
• IE
VOLATILE OR13ANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Keystone DCI 0600B --<>4-
_EPA SAMPLE NG
S-IO-FB<2-4l
C,,nt r a,: t: I 7'3230-04
L<1b C,:,de: kEYT X ,:ase No.: 06008 SAS N,o.: ____ SDG No.: C30WA
Matri•: (soil/w~terl SOIL
Sample wt/v,,l: 5.0 (g/mU §__
LOW
% Moisture: not dee.
C,:il umn PACK
Number TI(>s found: __ l
CAS NUMBER COMPOUND NAME
Lab Samp I e ID: '3•)06008 I 0
Lab File ID: 4U0600BVIO
Date Re,:eived: 06/0:?/'30
Date Analyzed: 06/0B/'30
Di 1 ut i ,on Fa,:tor: ~l~-~I) __ _
CONCENTF:A Tl ON UN ITS:
(ug/L ,,r ug/Kgl UG/KG
RT EST. CONC.:; Q
:=~-~--------------:----------------------------:--------:-------------:-----:
t. :UNKNOWN I. 70 : 7.0lJ
' ' '--------------------------------------------·--------
FORM I VOA-TIC 1/B7 Re
00021J
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• IE
VOLATILE OPGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Keystone DC• 06008 -<>-I-
EPA SAMPLE NO.
S-IO-FB<:-4D
Lab N~me: KEYSTONE ENV.
Lab Cc,de: kEYTX Case N1:,. : 06008 SAS N,o.: SDG No.: C30WA
Mat r i :,; : ('5,:,i 1 /w,3ter) SOIL
Sample wt /vol: 5. I) (g/mU §___
Level: ( l ,:,w/med) LOW
7. Moisture: not dee. 22
Column (pa,: k/,:ap) PACK
Number TICs f,:,und: __ I
CAS NUMBEF: COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Rei::ei ved:
Date Analy:ed:
Dilution f"acti,r:
CONCENTRATION UNITS:
(ug/L ,or ug/Kg) U13/KG
"300600811
4U06008V!:
06/02/90
06/08/"30
1.0
F:T EST. CONC •. : Q
: ~=======---==~-==: =-·----·--==--====-=----=====:==:==------:===========:st::====:
I. 7446-09-5 : SULFUF: DIOX !DE(ACN) (DOT) 1. 45 : 130 · : J
--------------------------------------------------------------------
rORl1 I VOA-TIC 1/87 Re,
000221
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••
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Keyst,,ne DCI 06008 --Q-1-
_E?A SAMPLE NC,
S-13A-FBIO-:::
Lab Name: KEYSTONE ENV.
Lab C,:,de: f'.EYTX Case N,:,.: 06008
Matrix: lsoll/~aterl SOIL
Sample wt/v,,l: ~ lg/mL) §_
Level: I lo~/med) LOW
X Moisture: not dee.
C•:. l umn (pa,:k/cap) PACK
Number TICs f,:,und: __Q
CAS NUMBER COMPOUND NAME
·---.
SAS N,:,.: ____ SDG No.: C30WA
Lab Samp 1 e IO: '3006008 I::'
Lab File IO: 4UOE,008V I:::
Date Re,:ei ved: 06/0::'/90
Date Analy=ed: 06/08/90
Di 1 u t i ,on Fact ,,r : I. 0 -'-'--"'-----
cmJCENTRA Tl ON UN ITS:
lug/Lor ug/Kgl UG/KG
F.:T EST. CONC.~ g
FORM I VOA-TIC 1/87 Re·
000231
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• IE
VOL1\TILE ORG1\NICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Key5tona DCI 06008 --04-
_EPA SAMPLE NO
S-13A-FB<:--i
L.,b Name,: KEYSTONE ENV.
Lab C,~de: KEY TX Case No.: OE.008
Matri~: (soil/water) SOIL
Sample wt/vol: 5.0 (g/ml) §__
Level: ( I ow/med J LOW
% Moisture: not dee. 22
Column (pack/o:.ap) PACK
Number T!Cs f,:iund: __Q
CAS NUMBER COMPOUND NAME
SAS N•:>.: SDG No.: C30WA
Lab Samp 1 e ID: 90<)6008 I 3
Lab File ID: 4U06008Vl3
Date Re,:eived: 06/02/'30
Date Analyzed: 06/08/'30
Dilution Factor: ~l~·~0'---
CONCENTRATION UN ITS:
(ug/L i:ir ug/Kg) UG/KG
RT
, ' 1 •
EST. CONC.· : ll
: -----------==:::==: ====------=------·------------: ---·-----: ============::-=: =====: : ____________________________________________ : ________ -----------:_: ____ _
FORl't I VOA-TIC 1/87 Re
000240
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• IE
VOLATILE ORGMIICS ANALYSIS DATA SHEET
TENT A Tl VEL Y I DENT! FI ED COMPOUNDS
Key§tone DCI 06008 ---04-
_EPA SAMPLE NO.
Lab Name: KEYSTONE ENV.
Lab Cc,de: KE\' TX
Matri": ls,oil/1.1ater:> SOIL
Sample wt/vol: 5.0
Level: ( 1 ,:,w /med) LOI~
'l. Moisture: not dee. 20
(pa,: 1-:: /,: ap) PACK
Number TICs found: __ I
CAS NUMBER
1. :UNKNOWN
X-1-0SN<O-:.>
Contract: 179280-1)4
(g/mU _G __
COMPOUND NAME
SAS N,:,.: SDG No.: C30WA
Lab 5.J.mp I c, ID: '300£008:2~
Lab Fi I e ID: -IUOE.0081/:::-?
Date Received: 0£/07/90
Date Analyzed: 0£/14/90
Di 1 ut i ,:,n F'ac t,:,r: .,_1.,_ • .:.<o __ _
CONCENTRATION UNITS:
(ug/L ,:ir ug/Kg) IJG/f(G
RT EST. CONC,~ Q
1.70 l II :;
---------------------------------------------------------------------
f"ORl1 I VOA-TIC 1/87 Re,
000249
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•
(
IE
VOLATILE OPGANICS ANALYSIS DATA SHEET
TENT,HIVELY IDENTIFIED COMPOUNDS
Key9tone DCI 06008 -04-
_EPA SAMPLE NO
X-3'3-EAlO-::J
L•b Name: KEYSTONE ENV.
Lab Code: KEYTX Case N,:,.: 1)6008
Ccntract: 17'3280-04
SAS No.: SDG N,:,.: C30WA
Matrix: (s,:,i 1 /w'ater) SOIL
Sample wt/vc,1: 5.1)
Level: < ! ,:,w/med) LOW
¼ Moisture: not dee. :o
Column (pack/,:ap) PACK
Number TICs found: __ !
CAS NUMBER
:UNY-NOWN
'
(g/mL) §__
COMF'OUND NAME
Lab Sdmple ID:
Lab File ID:
Date Re,: ei ved:
Date Analyzed:
Diluti,:in F"a,:tor:
CONCENTRATION UNITS:
( ug /L ,:,r ug /Kg) UG/KG
'300600814
4UOE.<)08V 14
06/02/'30
06/08/'30
1.0
RT EST. CONC. Q
1.70 :
I----------------------------------------------------------------------
fORM I VOA-TIC 1/87 RE
00025
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• IE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Keystone DCI 06008 --04-
_EPA SAMPLE NO.
X-46-WA Lab Name: KEYSTONE EN'J. Contract: 179:80-04
Lab C,ode: f!EYTX Case No.: 06008 SAS No.: SDG No. : C30WA
Matr i '" (s<)i I /water) SOIL
Sample wt /vol: 5.0 Cg/mL) G __
Level: (low/med) =L=O~W~-
¼ Moisture: not dee.
C,:.11 umn (pack/cap) PACK
Number TICs f,.:iund: ___d
Lab Sample ID:
Lab Fi le ID:
Date Re,:ei ved:
Date Analyzed:
Dilution tactor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
'30060081'3
4U06008V! 9A
06/06/'30
06/ I l/'30
1.0
CAS NUMBEF: COMPOUND NAME RT EST. CONC~-0
.:======----------:----------------------------:--------
:. 76-13-1
:UNKNOWN
:ETHANE, 1,l,2-TRICHLOR0-1,2,2:
:UNKNOWN
' '
1.70
7.40
24.50
'--------------------------------------------·--------
FORl't I VOA-TIC
18 J
46 J
'3.0 J
1/87 Re,
000269
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• lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Keystone DCI 06008 --04-
_EPA SAMPLE NO.
X-7-LF
Lab !tame: KEYSTONE ENV.
Lab C,:,de: f'.EYTX Case No.: 06008
c,,nt r a,: t : I 7":1280-04
SAS N.:,.: SDG No.: C30WA
Matrix: (soi I /•eater) SOIL
Sample wt/vol: 5.0
Level: ( I ,:,1o1/med) LOW
'l. Moisture: not dee. 23
C,:-1 umn (pack/cap) Pt.O'.
Number T!Cs found: __ I
CAS NUME<Ef.•
I. :UNl<NOWN
(g/mU §__
COMPOUND NAME
Lab Sample ID: 900600818
Lab File ID: 4U06008V I BA
Date Re,:ei ved: 06/06/90
Date Analyzed: 06/11/90
CONCENTRATION UNITS:
<ug /L .:,r ug /Kg) UG/1<'13
RT EST. CONC.:
1. 70 : 51 c :J
Q
f"ORl1 I VOA-TIC 1/87 Re-.
.000284
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VOLATILE OR(;ANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Key5tone Den 06008 -04-
_EPA SAMPLE NO.
L3b Name: KEYSTONE ENV.
Lab (:,:,de: KE'iT '.-: Case No.: 06008
Mat r i :,, : f s,:,i l /water) SOIL
Sample wt /vc,J: 5.0 (g/mL) §__
Level: ( 1 ,,,., /med) LOW
'l. Moisture: not de-:. _1Q
Column (pad:/cap) PACK
Number TICs f,:iund: __Q
CAS NUMBEF: COMPOUND NAME
X-93
SAS No.: SDG No,: C30WA
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Di l •Jt i ,:in rai:tor:
CONCENTRATION UNITS:
(ug/L ,or ug/Kg) UG/KG
':3006008::7
4U06008V'.:7
06/07/'30
06/14/'30
1.0
RT EST. CONC;; Q
FORM I VOA-TIC 1/87 Re
000294
..
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10 EPA SAMPLE NO.
PESTICIDE ORGANICS ~NALY515 DATA SHEET
s-so Lab Name: KEYSTONE ENV. Contract: 17·~280-04
Lab Code: I EYTX Case No. : (il:,(H)8 SAS No.: SDG No . : C30WA
Mat,-1 : (soi l/wate,-) SOIL Lab Sample ID : ·j(H)l:,8-1)1)5A
Sample wt/vol: 30.0 <g/mL) G Lab Fi le ID:
Level : (low/med) LOW
X Moisture: not dee. 10 dee.
Date Received: 06/01/90
Date Extracted: 06/06/91)
E~tract1on: ISepF/Cont/Sonc) SONC Date Analy:ed: 1)6/22/30
GF·C Cleanup: (Y/N) N cH: ':,.4 Dilution Factor: 1.00
CAS NO. COflFOUtJCr
CONCENTRATION UNITS:
(ug/L or ug/Kgl UG/KG
319-84-6--------alpha-BHC __________ _ 34 :x
31 ':1-85-7--------be,. a.-BHC __________ _ 8. ·:, :u 313-8b-8--------delta-8HC __________ _ 8.9:u
58-89-9---------gamma-BHC (Lindane> ____ _ 8. ·:-1 :u 76-~4-8---------Heptachlor _________ _ 32 :x 3,)·~-OO-2--------Aldrin ___________ _ 8. ·:t: U
1!)24-57-3-------Heptachlor epaxide _____ _ 8. "3 :u
95·:1-·:18-8--------Endosu l fan I ________ _ s.·:1:u ~0-57-1---------Dieldrin __________ _ 28 :x 72-55-9---------4,4'-DDE __________ _ 1S :u 72-20-8---------Endr in. ___________ _ 1S :u
33213-65-9------Endosulfan II ________ _ 38 :x
72-54-8---------4 ,4 '-DOD __________ _ 18 :u
1031-<)7-8-------Endo,;u l fan sulfate _____ _ 18 :u
50-29-3---------4,4'-DDT __________ _ 38 :x 72-43-5---------Metho:<ychlor ________ _ 89 :u
53494-70-5------Endrin ketone ________ _ 18 :u
5103-71-9-------alpha-Chlordane _______ _ 8"3 :u
5103-74~2-------gamma-Chlordane _______ _ 89 :u
S001-3~-.!-------Toxaphene __________ _
12b74-11-2------Aroclor-!Olb ________ _
180 :u
8·, :u
11104-28-2------Aroclor-1221 ________ _ 8'3 :u
11141-16-~------Aroclor-1232 ________ _ 8"3 :u
534&'3-21 -·3------Aroc 1 or-1242 ________ _ 89 :u
12b72-29-b------Aroclor-1248 ________ _ 89 :u
11 •)'~7-~-·3-1------Aroc l or-1254 ________ _ 180 :u
110':-16-82-5------Aroc l or-1261) ________ _ 180 :u
FORM I PEST
Q
001'133
1/87 Rev.
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ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: KEYSTONE ENV. Contract: 17~280-04 X-1-0SN(0-2>
Lab Code: KEVTX Case No. : 01:-00S SAS No.: SDG No. : C3<)WA
Mat,-i,: <soi \/water) SOIL Lab Sample ID: 90068-02~A
Sample wt/vol : 3<).0 (g/mU G Lab Fi le ID:
Level : < low/med l LOW
¼ Moisture: not dee. 20 dee:.
E:<t1-ac:t ion: (SepF/Cont/Sonc:l SONC
Date Received: 06/06/iO
Date Extracted: 06/11/90
Date Analy:ed: 06/23/~0
GPC Cleanup: IV/NI N pH: 3.7 Dilution Factor: 1.00
CONCENTRATION UNITS: CAS NO. COMFOUN[, Cug/L or ugi~·g) UG/k:G Q
31S-24-~.--------alpha-8HC __________ _ 1 (J :u
319-S5-7--------beta-BHC~----------
31S-86-8--------delta-8HC __________ _
10 :u
1 (l :u 58-89-9---------gamma-BHC (Lindane) ____ _ 10 :u 76-44-8---------Heptachlor _________ _ 10 :u
31)~-00-2--------Aldr1n~----~------
1024-57-3-------Heptac:h\o,-epoxide _____ _
I I) :u
10 :u ·~5~-SS-8--------Endosulfan I ________ _ 10 :u
E,i)-57-1---------Dieldrin -----------20 :u 72 -55 -9 - - - - - - - - -4, 4 ' -DD E __________ _ 20 :u
72-20-S---------Endi-in~-~~--------
33213-65-·~------Endosulfan II ________ _
72-54-8---------4,4'-DDD __ -,-_______ _
1031-07-S-------Endosu\fan sulfate _____ _
2<) :u
20 :u
20 :u
20 :u 50-29-3---------4,4'-0DT __________ _ 20 :u 72-43-5---------Methoxychlor ________ _ 100 :u
53494-70-~------Endrin ketone ________ _ 20 :u 5103-71-9-------a\pha-Chlordane _______ _ 100 :u 5103-74-E-------oamma-Ch\ordane _______ _ 100 :u
8001-3~~2-------Toxaphene.,---:----------
12674-11'-2------Aroc: lor-1<)1€. ________ _ 200 :u
100 :u 11104-28~2------Aroclor-1221 ________ _ 100 :u 11141-16-5------Aroc:\or-1232 ________ _ 10•) :u
534€.9-21-9------Aroc:lor-1242 ________ _ 100 :u 12€.72-29-6------Aroc:lor-1248 ________ _ 100 :u
110-:<7-E-·~-l ------Aroc: lor-1254 ________ _ 2(>0 :u
110'3t:.-82-5------Aroc: l or-121:.<) ________ _ 200 :u
---
001443
FORM I PEST 1/87 Rev.
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I [I EPA SAMPLE NO.
PESTICIOE ORGANICS ANALYSIS DATA SHEET
X-93
Lab Name: KEYSTONE ENV. Contract: 179281)-04
Lab Code: KEYTX C.ase No.: SAS No. : S(•G No. : C30WA
Matri:,-,:: (soi !/water) SOIL
Sample wt/vol: 30.0 (g/mU G Lab File ID:
Level: (\ow/med) LOW
¼ Moisture: not dee. 10 dee.
Date Received: OE./Ot:J·:fO
Date Extracted: 06/11/90
<SepF/Cont/Sonc) SONC Date Analv:ed: 06/23/90
GF'C CleanL•D: CY /N) N pH: 6.3 Dilution Facto•·: 1 .(10
CONCENTRATION UNITS:
CAS NO. COMF·OUND Cug/L or ug/Kgl UG/KG Q
319-84-6--------alpha-BHC _________ _ 8. ·:f: U
319-85-7--------beta-BHC __________ _ s.9:u
319-86-8--------delta-BHC -----------8.9:u
58 -89 -9 - - - - - - - - -gamma -8 H C <Lindane) ____ _ S.·:f:U
76-44-8---------Hep\ach\or _________ _ s.·; :u
3<)9-c)0-2--------Aldrin ___________ _ a.-;-:u
1024-57-3-------Heptach\or epoxide _____ _ s.s.:u
~5~-93-8--------Endosu\fan I ________ _ 8. ·j: U
61)-57-1---------Dieldrin __________ _ 18 :u
72-55-9---------4,4'-DDE __________ _ 18 :u
72-20-8---------Endrin ___________ _ 18 :u
33213-~5-9------Endosulfan II ________ _ 13 :u
72-54-8---------4,4"-DDD __________ _ 18 :u
1031-07-8-------Endosu\fan sulfate _____ _ 18 :u
50-29-3---------4,4"-DDT~----------72-43-'5---------Me\hoxych\or ________ _
13 :u
8"3 :u
53494-70-5------Endr,n ketone ________ _ 18 :u
'5103-71-9-------a\pha-Ch\ordane _______ _ 39 :u
'51•)3-74-2-------gamma-Ch \ordane _______ _ 89 :u
8001-35-2-------Toxaphene __________ _ 180 :u
121:>74-11_-2------Aroc \or-101 ; ________ _ 8'3 :u
11104-28-2------Aroc\or-1221 ________ _ 89 :u
11141-16-5------Aroc\or-1232 ________ _ 8'3 :u
53469-21-9------Aroc\or-1242 ________ _ 8"3 :u
12672-29-J:>------Aroc\or-1248 ________ _ 89 :u
11097-69-1------Aroc\or-1254 ________ _ 180 :u
11096-82-'5------Aroc\or-1260 ________ _ 180 :u
001458
FORM I PEST 1/87 Rev.
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--·---.
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET EF·A SAMPLE NO.
Lab Name: KEYSTONE ENV. Contract: 17~280-,)4
SAS No. : SDG No. : C3•)WA
Lab Sample ID: ~1)068-02SA
Sample wt/vol: 30 .0 <glmU G
LOW
Lab Fi le ID:
Level: < \ow/med i
¼ Moisture: not dee. 8 dee.
Date Received: 06/06/<;Q
Date Extracted: 06/11/90
Date Ana\y:ed: 06/23/90 Extraction: <SepF/Cont/Soncl SONC
GPC Cleanup: <YIN) N pH: Dilution Factor: I .00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kgl UG/KG Q
31·~-84-6--------alpha-BHC ___________ _ 21 : X
319-85-7--------beta-BHC--,-___________ _
319-86-8--------delta-BHC~-----------
58-89-·~---------9amma-BHC (Lindane) _____ _
8.7:u
8.7:u
2.1:u 76-44-8---------Heptach\or __________ _ 22 :x
31)~-(10-2--------Aldrin _____ ~-------
1024-57-3-------Heptachlor epoxide _____ _ 8.7:u
s.1:u ~59-98-8--------Endosulfan ! _________ _ s.7:u
60-57-1---------0ieldrin ___________ _ 17 :Jx 72-55-9---------4,4'-DDE ___________ _ 17 :u
72-20-8---------Endrin ____________ _ 17 :u
33213-65-9------Endosulfan II ________ _ 21 : X 72-54-8---------4,4'-DDD ___________ _ 17 :u
1081-07-8-------Endosulfan sulfate _____ _ 17 :u
50-29-.3---------4 ,4 '-DDT ___________ _ 21 :x
72-43-5---------Methoxychlor _________ _ 87 :u
53494-70-5------Endrin ketone ________ _ 17 :u
5103-71-9-------a\pha-Ch\ordane _______ _ 87 :u
5103-74-2-------gamma-Ch\ordane _______ _ 87 :u
8001-3~-2-------Tox~phene ___________ _ 170 :u
12674-!l-2------Aroc\or-!OIG ________ _ 87 :u
11104-28~2------Aroc\or-1221 ________ _ 87 :u
11!4!-lb-5------Aroc\or-!232 ________ _ 87 :u
53469-21-9------Aroc\or-!242 ________ _ 87 :u
12672-29-6------Aroclor-!243 ________ _ 87 :u
110"37-69-1------Aroc \ or-1254 ________ _ 170 :u
11 o·~E,-82-5------Ar oc I or-1260 _________ _ 170 :u
0.01163
FORM I PEST 1/87 Rev.
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1D EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
Lab Name: KEYSTONE ENV. Contract: 179230-04
Lao Code: f,.EYTX Case No. : Of:,(H)8 SAS No.: SDG No. : CSOWA
Matri::::: (sol l/water> SOIL lab Sample ID: ~c)068-1)l~A
Samp le wt/vol : 30 .(l (g/mL> G Lab Fi le ID:
Leve I: (\ow/med) LOW Date Received: 0~/1:16/90
¼ Moisture: not dee. 20 dee. Date Extracted: 06/07/90
Date Analy;:ed: (lf:./23/·::HJ E~traction: <SepF/Cont/Sonc) SONC
GF'C Cleanup: <YIN> N pH: 4,5 Dilution Factor: l .00
CAS NO. COMPOUND
CONCENTRATION UNITS:
<ug/L or ug/Kg) UG/KG
319-8~-s--------alpha-BHC ___________ _
319-35-7--------beta-BHC ___________ _
31"3-86-8--------delta-BHC ___________ _
58-8~-9---------gamma-BHC (Lindane> _____ _
16-44-8---------Heptachlor __________ _
30·~-00-2--------A ldr in ____________ _
1024-57-3-------Heptachlor epoxide _____ _
959-98-S--------Endosulfan I _________ _
f:.0-57-1---------Dieldrin ___________ _
72-55-9---------4,4'-DDE ___________ _
72-20-8---------Endrin _____________ _
33213-65-3------Endosulfan II ________ _
72-54-8---------4,4'-DDD ___________ _
1031-07-3-------Endosulfan sulfate _____ _
50-29-3---------4,4'-DDT ___________ _
72-43-5---------Methoxychlor _________ _
53494-70-5------Endrin ketone ________ _
5103-71-9-------alpha-Chlordane _______ _
5103-74-e-------9~mma-Ch\ordane _______ _
8001-35-S-------Toxaphene ___________ _
l 2b74-11'-2------Aroc \or-1(11& ________ _
11104-28-2------Aroclor-1221 ________ _
11141-16-5------Aroc\or-1232 ________ _
534(,9-21-3------Aroclor-l242 _________ _
12072-29-b------Aroclor-1248 ________ _
11097-E,9-l ------Aroc l or-1254 _________ _
110'36-82-5------Aroc I or-1260 _________ _
10 :u
10 :u
10 :u
1 I) : U
10 :u
10 :u
10 :u
0.84:JX
2<) :u
20 :u
t.4 :Jx
20 :u
20 :u
20 :u
3 .2: JX
1(11) :u
20 :u
100 :u
100 :u
20<) :u
100 :u
100 :u
100 :u
100 :u
100 :u
200 :u
200 :u
Q
001448
FORM I F'EST 1/87 Rev.
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lD EF'i< SAMPLE NG.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
X-7-LF
Lab Name: KEYSTONE ENV. Contract: 17·:'28(1-1)4
Lab Code: f.EvTX Case No • : (lf:,1)(18 SAS No.: S(1G No. : C30WA
Mat,-i:,,,:: (soi l/wateri SOIL Lab Sample ID: 90c)~8-,)18A
Sample wt/vol: 3(1 .0 (g/mL) G Lab File ID:
Leve\: ( \ow/med) LOW Date Received: 1)6/06/90
¼ Moisture: not dee. 23 dee. Date Extracted: 06/07/90
E:<tract ion: (SepF/Cant/Sonc)
<YIN) N
SONC Date Analyzed: 06/23/·:"11)
GPC Cl eanL1p: pH: 3. 7 Dilution Factor: 1 .01)
c.:.s NO. CGMF·OUN(1
CONCENTRATION UNITS:
<ug/L or ug/Kgl UG/KG
31~-84-~--------alpha-BHC __________ _
31'~-85-7--------beta-8HC ___________ _
31'~-SE,-8--------delta-BHC -----------58-8~--~---------qarnma-8HC <Lindane) _____ _
7~-44-8---------Heptachlor __________ _
309-1),:,-2--------Aldrin ____________ _
11)2'1-57-3-------Hep t ach \ a,-epo" i de ------~59-~8-8--------Endosulfan ! _________ _
~0-57-1---------Dieldrin ___________ _
72-55-9---------4,4'-DDE ___________ _
72-20-8---------Endrin ____________ _
33213-~5-9------Endosulfan II ________ _
72-54-S---------4,4'-DDD ___________ _
1031-07-B-------Endosulfan sulfate _____ _
50-29-3---------4,4'-DDT ___________ _
72-43-5---------Methoxychlor _________ _
53494-70-5------Endrin ketone ________ _
5103-71-9-------a lpha-Ch lordantt _______ _
5103-74-2-------gamma-Chlordane _______ _
8001-3~-2-------Toxaphene.,--,----------
12&74-11-2------Aroclor-1016 ________ _
11104-28-2------Aroclor-1221 ________ _
11141-1&-5------Aroclor-1232 _________ _
53469-21-9------Aroc\or-1242 _________ _
12672-29-6------Aroclor-1248 _________ _
11097-69-1------Aroclor-1254 _________ _
11(1·~6-82-5------Aroc lor-1260 _________ _
1 (l :u
13 :x
10 :u
10 :u
1 (, :u
I) .2·i,: JX
10 :u
10 : U
21 :u
21 :u
21 :u
21 :u
21 :u
21 :u
0.92:JX
100 :u
21 :u
100 :u
100 :u
210 :u
1<)0 :u
100 :u
100 :u
100 :u
100 :u
21•) :u
210 :u
Q
---
001153
FORM I PEST 1/87 Rev.
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ID EPA SAMPLE NO. F·ESTICl[IE ORGANICS ANALYSIS DATA SHEET
X-RINSATE Lab Name: KEYSTONE ENV. Contract: 179280-04
Lao Code: 1.EYT X Case No. : 06008 SAS No . : SDG No. : C30WA
Sainp t e wt I vo 1 :
WATER
100<) (g/mU ML
LOW
Lab Sample ID: 90063-0!6A
Lab Fi le ID:
Level: (low/med)
XMoisture:notdec. dee.
Date Received: 1)6/02/":10
Date Extracted: 06/04/90
Date Analy:ed: 06/22/90 Extraction: <SepF/Cont/Sonc) CONT
GF'C Cleam,p: <YIN) N pH: 4 .5 Di tut ion Factor: I .00
CONCENTRATION UNITS:
CAS NO. COMF·OUND <ug/L or ug/Kg) UG/L Q
319-84-6--------~lpha-BHC __________ _
31·~-85-7--------beta-BHC __________ _
31·~-SE--8--------delta-BHC __________ _
58-89-~---------gamma-BHC (Lindane) ____ _
76-44-8---------Heptachlor _________ _
30·:l-(H)-2--------A l dr in ___________ _
11)24-57-3-------Heptachlor epoxide _____ _
959-·~8-8--------Endosulfan I ________ _
60-57-1---------Dieldrin, __________ _
72-55-·~---------4,4'-DDE __________ _
72-20-8---------Endr in, ___________ _
33213-65-9------Endosulfan II ________ _
72-54-8---.------4 ,4 '-ODD __________ _
1031-07-8-------Endosulfan sulfate _____ _
51)-29-3---------4,4'-DOT __________ _
72-43-5---------Methoxychlor ________ _
53494-70-5------Endrin ketone _______ _
SI 03-71 -·:1-------a lpha-Ch lordane _______ _
5103-74-2-------gamma-Chlordane ______ _
8001-35-2-------Toxaphene __________ _
12b74-11~2------Aroclor-lOI& ________ _
11104-28-2------Aroclor-1221 ________ _
11141-16-~------Aroclor-1232 ________ _
534E,:1-21-9------Aroclor-1242 ________ _
12672-29-6------Aroclor-1248 ________ _
11097-b9-1------Aroclor-1254 ________ _
11 o·~f:,-82-5------Aroc lor-12bV ________ _
() ,(15t) :U
o.1:i50:u
0.050:U
I) .051) :u
c,.05,):u
1). 050 : U
(J .051) :u o.oso:u
0. 10 :u
0.10:u
9 .10 :u
0.10:u
0. 11) :u
0.10:u
0 .020: JX
o.5o:u
0. 1<) :u
o.so:u
o.so:u
1.0:u o.so:u o.so:u
0.50:u o.so:u o.so:u
1 .o :u
1.0:u
-,
'
001468
FORM I PEST 1/87 Rav.
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ID EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
X-RINSATE Lab Name: ~EYSTONE ENV. Contract: 179230-04
SAS No. : SDG No. : C3<)WA
Mati-i:.-,:: <s01 l/wate,-) WATER
Sample wt/vol: 1 !)()(I (g/mll ML Lab Fi le IC<:
Level: ( I ow/med l LOW
:,: Mais t u1-e: not dee. dee.
Date Received: O~/()~/·~o
Date Extracted: 06/0~/90
E:-:t1-act ion: <SepF/Cont/Sonc) CONT Date Analyzed: 06/23/90
GPC CleanLtD: (Y /Nl N pH: 7.0 I)ilution Factor: 1.(u)
CAS NO. COMPOUNC<
CONCENTRATION UNITS:
<ug/L or ug/Kgl UG/L
319-84-6--------alpha-8HC __________ _
31·~-85-7--------beta-BHC __________ _
319-86-8--------delta-8HC __________ _
58-83-·~---------gamma-BHC (Lindane) ____ _
76-44-8---------Heptachlor _________ _
S(i~-Or)-2--------Aldrin, ___________ _
1(124-57-3-------Heptachlor epo):ide _____ _
35~-98-8--------Endosulfan I ________ _
6(1-57-1---------Dieldrin __________ _
72-55-9---------4.4"-DDE ________ _
72-20-8---------Endrin, ____________ _
33213-~5-9------Endasulfan II _______ _
72-54-8---------4,4"-DDD __________ _
1031-07-8-------Endosulfan sulfate _____ _
50-23-3---------4,4'-DDT __________ _
72-43-5---------Methoxych\or ________ _
534'~4-70-5------Endr in ketone ________ _
51<)3-71-9-------a \pha-Ch \ordane ______ _
5103-74-2-------gamma-Chlordane _______ _
8001-35-2-------Toxaphene ________ __,_ __
12674-11-2------Aroc\or-1016, ________ _
11104-28-2------Aroc\or-1221 ________ _
11141-1&-S------Aroclor-1232 ________ _
53469-21-9------Aroclor-1242 ________ _
12672-29-6------Aroclor-1248, ________ _
110':'7-E.9-1------Aroc \ or-1254 ________ _
1 l(,.~E.-82-5------Aroc I or-126<) ________ _
(). 051): u
0 .OS•) :u
0 .051) :u
O.O.Sc):u
() .c)51) :u
o.oso:u
0.050:u
(.1.1)5(1 :u
0.10:u
0.10:u
0.10:u
0. l(J :u
0.10:u
0.10:u
0.10:u
<).5<) :u
0.10:u o.so:u
0.5<) :u
I .0 :u o.so:u o.so·u o.so u o.so u
0.'30 U
I .0 U
1.0 U
Q
l
I
:
001473
FORM I PEST t/87 Rev.
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10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
X-RINSATE
Lab Name: ~EYSTONE ENV. Contract: 179281)-04
Lab Code: 1.EYTX Case No. : (l~.1)1)8 SAS No. : SDG No. : C3<)WA
Mat,·,:.: (soi \/wate1·) WATER Lab Sample ID: ·~OO68-<)26A
Sample wt/vol: 1000 <glmLl ML Lab File ID:
Leve\: <low/med) LOW
X Moisture: not dee. dee.
Date Received: 06/0~/90
Date Extracted: O~/(19/9O
Date Analyzed: 06/23/90 E.:0.t1-act ion:
GF·C C\eanL1p:
(SepF/Cont/Soncl
(Y/Nl N
CONT
pH: 7.5 Dilution Factor: I .00
CONCENTRATION UNITS:
cA;; r,o. COMF·OUN[I lug/Lor ug/Kgl UG/L Q
319-8~-&--------a\pha-8HC __________ _
31~-85-7--------beta-BHC __________ _
31'~-86-8--------delta-BHC __________ _
58-8'~-~---------gamma-BHC \Lindanel ____ _
76-44-8---------Heptachlar _________ _
3()9-01)-2--------Aldrin ___________ _
11:124-57-3-------Heptachlor epo~<ide _____ _
-~59-98-8--------Endosulfan I ________ _
60-57-1---------Dieldrin __________ _
72-55-9---------4,4'-DDE __________ _
72-2O-8---------Endrin ___________ _
33213-65-9------Endosulfan II ________ _
72-54-8---------4,4'-DOD __________ _
1031-07-3-------Endosu\fan sulfate _____ _
50-29-3---------4,4'-DOT __________ _
72-43-5---------Methoxych\or ________ _
534':14-70-5------Endr in ketone ________ _
5103-71-9-------alpha-Ch\ordane _______ _
5103-74-2-------gamma-Chlordane _______ _
80<) 1-35-2-------Toxaphene __________ _
12b74-11~2------Aroclor-1016 ________ _
11104-28~2------Aroc\or-1221 ---------11141 -16 ~ ~ - - - - - -Aro c \or -1232 ________ _
534b9-2!-9------Aroc\or-1242 ________ _
l 2~,72-29-6------Aroc \or-1248 ________ _
11097-b9-1------Aroc\or-1254 ________ _
110%,-82-5------Aroc \or-I 2b0 ________ _
l) • 1)(> 1 ':I : J X
1).(iso:u
0.050:U
o.oso:u
() .0!50 :u
o.c:iso:u
0.050:U
o.oso:u
o.1c1:u
0. 1 (> :u
c).10:u
0.10:u
0. 10 :u
0.10:u
0. 10 :u
0.50:U
0.10:u
o.so:u o.5o:u
1 .c): U
o.so:u o.so:u
o.so:u o.so:u
o.so:u
I .0 :u
1.()!U
001178
FORM I F'EST 1/87 Rev.
.-
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ID EPA SAMPLE NO. PESTICIDE ORGANICS ANALYSIS DATA SHEET
S-FdNSATE
~ab Name: ~~-,STONE ENV.
SAS No.: SDG No. : C30WA
Lab Sample ID: 901:J63-015A
Sample wt/vol: 1000 <gimU ML Lab Fi le ID:
Level : <low/med) LOW
¼ Moisture: not dee. dee.
Date Received: OEJ02/91)
Date Extracted: 06/04/90
Date Ana\y:ed: 0&/22/90
Dilution Facto,-: 1.<)0
<SepF/Cont/Soncl CONT
GFC Cleam1p: (Y/N) N pH: <1.t)
CAS NO. COMF'OUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
319-84-6--------alpha-BHC ___________ _
319-85-7--------beta-BHC ___________ _
31·~-86-8--------delta-BHC ___________ _
58-89-3---------gamma-BHC Clindane) _____ _
76-44-8---------Heptachlor __________ _
309-00-2--------Aldrin ____________ _
102Q-57-3-------Heotachlor eooxide _____ _
·35·3-98-8--------Endosulfan I _________ _
~.,)-5"7-1---------Dieldrin ___________ _
72-55-9---------4,4'-DDE ___________ _
72-20-8---------Endrin ____________ _
33213-65-9------Endosulfan II ________ _
72-54-8---------4,4'-DDD ___________ _
1031-07-8-------Endcsulfan sulfate _____ _
51)-29-3---------4,4'-DDT ___________ _
72-43-5---------Methoxychlor _________ _
534':i4-70-5------Endr in ketone ________ _
5103-71-9-------a\pha-Ch\ordane _______ _
5103-74-e-------gamma-Ch \ ordane _______ _
8001-35~.S-------Toxaphene_...,... ________ _
12&74-ll~e------Aroclor-1016 ________ _
11104-28-e------Aroclor-1221 ________ _
1114!-1G-5------Aroclor-123e ________ _
53469-21-9------Aroc\or-1242 ________ _
12~-72-29-G------Aroc \or-1248 ________ _
11097-&9-I------Aroc\or-1254 _________ _
11 O·:ft.-82-5------Aroc l or-1260 _________ _
c) .050 lU
(J .1)51) :u
_o.oso:u
0.050:u
o.oso:u
0.050tU
I) .1)51) :u
0.()50:U
0 .10 :u
(1.10 :u
0. 10 :u
0 .10 :u
0.10:u
O.l(J:U
0.10:u
0.50:u
o. 10 :u
0.50:U
0.50lU
1 .o :u
0,50lU
0,501U
0.50iU
0.50iU
o.so:u
1 .o :u
1 .o :u
Q
., ..
001438
FORM I PEST 1/87 Rev.
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lF
SEM!VOLAT!LE OPGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
l'E'/S 70NE EN'!.
S.~mol e wt /v.:il:
~: Moisture: not dee. de,:.
E:. tr.:..,: ti. ,:,n:
l:JF'( Cle~nup: (Y/N) L pH: 7.0
CAS NUME<EF: COMPOUND NAME
I. 10544-50-0: SULFUF:, MOL. !"SB)
: IJM<NOlJN
Lab Fi le ID:
Date E,tracted: 06/09/9C
Dilution Factor: ~1~-~0 __ _
CONCENTPAT!ON UNITS:
(L19/L or ug/►:~g) U13/L
. :
F:T EST. CONC:
::.::::. 77 :
2"3, 71 : 37 :J
----------------------------------------------------------------------
000631
FORM I SV-TI C 1/67 Re
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1,,.., ... "I•
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SEN I \/QL1\ TI LE OF:(j,\N I 1: 3 ,;N,.\L 'ISIS D~ T/\ SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SDG N,:,. : ( 3('w,:.
Sample 'w't ,'v,:,l : Lab File ID:
(low/med) L=O~W~-
% Moisture: not dee. de,:. Date Extracted: 06/09/90
E:•, t ra.,: ti ,:,n: ( SepF / C,:,n t /S,.:,n,: ) CO!'lT Date Analy:ed: <:,6/20/90
6F'C: Cleanuo: pH: Dilution factor: ~1~-~0 __ _
CONCENTPATJON UNITS:
(ug/L or ug/Kg) UG/L
CAS NUMBEF: COMPOUND .'JAME
1.
-,
..;.
:ALIPHATIC COMPOUND
321-28-8:BENZENE, l-FLUOP0-2-METHOXY-:
: F'HTHALATE
:UMMO~JN
l":T
4.45
6.47
:20.89
·.:-·?. 7·-::.
EST. CONC;
•-L3:J
s.e:.;
6. 7:J
56 : J
----------------------------------------------------------------------
FORM I SV-TIC 1/87 Re
000643
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11
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AWD Technologies, Inc.
APPENDIX B
TENTATIVELY IDENTIFIED COMPOUNDS (TICS)
I
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!F" f:eyst,:,ne DCtt 06008 -: .. -=:
SEM!VOLAT!LE OPGANICS ANALYSIS DATA SHEET _EPA SAMP~~ NO.
TENT A TI ',ELY I DENT IF" I ED COl1F'OUNDS
S-10-F"E · -:-:.,
L.1b Sample ID: ·:'(H)6(H)8t)""7
Sample ,...,t/v,:,l: 20.0 <glmLJ ,.d...__ Lab F" i I e ID: 4U(l6()08(L'-:
Level: (1,:, .... /med) ~L~□~W~-
;: M,::iisture: n,:,t de,:. 34 de,:.
pH: 5.4
CMS l'JUMBEF COMF·DUND NAME
D.1t e Re,:ei ved:
Date E.xtra•:ted:
CONCENTPAT!ON UNITS:
(ur;;/·L ,:ir ug/kg) Ut~/kG
1)5/<):2/"3(,
1)6/c)E,,''j()
' EST. CONC.:
:1ETONE 3.38 240 :J
Q
:ALIPHATIC COMPOUND 4.::3 4300 :J ' ~ r. ---11.c;-:;,.;· 3:;-.;c1 ·e;a··....;,2c,•.c;·.:e--· -.r~· E'"''-l'l'TA" l',P ilf8H>,~l[,-.1~41-+I .'-'I" 1'fEM'FOl8;..Xx.¥V~-4>M~Eo'Tt+: ---'1h,,-!8.;::;;., -+----llf--'IH<'><) 18-) t8<) f)----+B. :..:.... 1
4. :ALIFH,\TIC HYDF:OCAF:80N 4.'3:2 :210 : J
5. : i..!N~·:.NOWN I:,. 07 1 :2!)0 : J .
E,. :H,\LO(jEN,\TEDH'IDPOCAF80N 5.38 430 :J
7
8.
'3.
l ').
11.
I.-.
13.
14.
I 5.
15.
I 7.
18.
: F ET ONE E,. 83 :2500 , "
:UNKNOWN 7.78
: UNf::NOWN
:UNl".NOWN
:ALIPHATIC COMPOUND
10544-50-0:SULFUR, MOL. 1581
: UN~;NOWN
: POL YAROMAT IC HYDF:OC,\F:BON
:UNKNOWN
:UNKNOWN
:UNKNOWN
:UNKNOWN
·::1.·3-::
:::::.:. ()5
23. ':15
·::5.51
:·3. 8:2
30.:24
33.77
34.04
850
1000
:so
1300
1 ·,00
:300
'300
2'300
I O<)C)
E,7C)
780
:J
:J
:J
:J
:BJ
:J
:J
:J
----------------------------------------------------------------------
FORM I SV-TIC 1 /87 Re·
000731
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.... ~-~ ..
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IF Keystone DCM 06008 -~J-E
SEMI '/OLA TI:..:=: OF:1;,.\N I C'3 AIIALYS I 5 DATA SHEET
TE,'H ;, T ! '.'ELY IDENTIFIED ,:.OMF·OUNDS
_EF'A S-"MFL~ NO.
s-10-re,, >4 •
SMS :J,:,.:
Level:
de,:.
E:,.tra,:t i,:,n:
r~F'C C 1 eanuo: 1 'r' / N) ~ pH:
Number TI(3 f,:,Ltnd: __l±
( ,.;5 NUME:EF COMPOUND NAME
:ALIPHATIC COMPOUND
:ALIPHATIC COMPOUND
3.
4.
1:.:.3 •..:: :.:.1:.:. rcrn,,,~,or.:c, l IP,'BFOA'/
8.
·3.
l (l.
II.
I :: •
13.
14.
: UNl:Nrnm
:ALIPHATIC COMPOUND
: PHTH1\L,\ TE
: F'HTHALA TE
: F·HTH1\LATE
: F·HTHALATE
:PHTHALATE
:PHTHALATE
:PHTHALATE
:PHTHALATE
: F·HTHALATE
i......c1b S ... 1mo le ID: '300E.;:,c)81 <-
Lab File ID: 4UOE.(i08C 1,:·
Date Pe,:eived: 06/0:C/'30
Date Extra,: t ed: f)E,/(1E,/·30
Dilution Pactor: LIL·~•l~O~--
CONCENTRATION UNITS:
•1.11::;/L ,:,..-u,;i.-T.g:: u1~,'~·:13
r
RT EST. CONCot
3. s:.: 570
4. I :: 1 E,(H)
t~ET I I. 73 53(0(:
E,. 05 53(J
6.37 :20(\
:.:'3. 54 E..S(•
::·3. 74 t,-:,:(1
·::·3. SI 1300
30.07 '3150
30. ! -~ 1-.:-00
30.:26 1500
30.41 16<)0
30.47 '3<)0
30.61 470
:J
:J
I E :•
:J
:J
:J
:J
:J
:J
:J
:J
:J
:J
:J
19 :
----------------------------------------------------------------------
FORM I SV-TIC I /87 Re,
000760
I
I
I
I
I
I
I
I
I
I
I
I
I
I
:1
I
I
.,.. ~-'\1.
I
I
lF
SE~! \.'OLA T: L~ OF1:J,.\/'l ~ 1:.~ ~N,!,l.. Y:3 ~ S C·A T ,~ Si--lCET
TENTAT!VELi '.DENT:FIED COMPOUNDS
Sa.mp le 1w,,1t /v,:,l: 30.(l (g/mi.....) §__
Levi: 1 :
% M(•isture: not dee. de,:.
E:.;t; r ..J.,:: i ,:,n:
6F'C CleanLtp: c.Y/N) t:L_ pH:
SONC
4.6
Lab File ID:
CON1:EtJT= ,-; T: ON IJN I TS:
(ug/L ,:,:"" 1_:9/t~g:1 U1:J/h:G
s-1i:,re, :.--! • s
,:,;s NUMBE,· ,::OMF'OUNO NAME EST. CONC.
I. : AL!F'HATlC cor~POUNO 3.47 ·.:40 . . ' -· -. :AL!F'H,',TI1: COMF'OIJNO 3.85 70(1 : J
3. :UNl'NOWN 4.33 ·j/r) :J 1J .·J. 1 -,:, I -·:I:_ F C?IT,\P40PJC, I I lYCFtJ.CY f1ET; 4.38 -. J(,t . (• '~-"J:•
~ : UNI NOI.JN 6.08 ·? 1 (J ;J
"'· : kETONE 6.81) E, '.2r) :J
: UIJI NOWN 7.77 :.:61) : J
8. : AL IPHATI1: COMF·OUND :::.::. (H) :.::(H) :J
·j • :PHTHALATE :.::·:1. 54 E,4(1 :J
1 (I. :PHTHALATE ·:_"j. 7:.:: 55(1 :J
I I. : F'HTHALATE .::·3. 8 I 1500 :J
1 ., :PHTHALATE -::·3. ·37 15(H) :J
13. :PHTHALATE 31).l)E, ':130 :J
H. :PHTHALATE 30.17 1 ·::1)1) :J
15. :PHTHALATE 30.::6 1500 :J
1 E,. !PHTHALATE 30.3:: 7'21) :J
I 7. !PHTHALATE 30. 3'3 870 :J
18. -~ !PHTHALATE 30.46 881) :J
1 8. :PHTHALATE 30. 5'3 470 :J
000783
FORM I SV-TIC I /87 Re,
I
I
I
I
I
I
I
I
I
I
I
.I
I
I
I
I
I
I
I
lF ~::L:?yst,:,ne DCtt OE,(H)8 -: ...1-
SEM ! •;OL,H I !..E O!'·,:,,;~JI CS ,;:siAL 'fS I 5 DAT A SHEC:T 'c:F ,; SA~F -~ : :O
TE,'iTATl'/ELY IDENTIFIED ,:OMF·OIJtJDS
Lab F"i le ID: ➔U0513t.1:.1::
Date Re,:eived: 06/0~/90
de,:.
6F'C Cleanup: fY/N) N oH: 4.7 D 1 l u ti ,:,n F' a,: t ,:,r : ! , (JC) ~-"-"--
COMPCIJND NAME
,:.ON•:EMTF:1, T ION IJN I TS:
,·1.1,;/L ,:,r u9/L:9) U(:l;T:j
F:T EST. CONC.
: ==•~====,,========: ========c~===================: ========: =============: ==-~.:;-.1
: ~-•,.:s .. :. .::.:. i[r~r,,~~o,~E, t 11'.'0F.OY.'/ 1 r1ETI 1.50 l 33('( 10:· 1
: ·.::. : UNLNOWN : ·j. l :2 : 1 ':J()() : J . ;
3. : UNf,'NOWN 1 S. 20 31 (i : J
-l. : ALIPHATIC HYDF:OCAF:BON 18. ·35 E,7(1 :J
~ :ALIPHATIC HYOF:OCAF:BON 1 ·:f. 02 :.:oo :J ~-
E,. : ,\L I F'H1, T I,: COMF'OUNO ·::::.:. 04 380 :J
~ 1!)544-Si)-1):SULFUP, MOL. rSS) ::2. ·:J? 44(H) :J
3. :UNKNOWM "23.37 :.::ao :J
·3. :UNl•NOWN :.::3. £:.: 710 :J
1 (J. : ALI F'HA TIC HYOF: □,:AF'BON :27.-1-1 4-1 I) :J
1 1. : ALIPHATIC HYDPOCAF'BON ::a.s: -110 :J I., :UNKNOWN :29. 17 ::GO :J
13. :UNKNOWN :::·3. 84 11 <)I) :BJ
14. :UNKNOWN 30. ·:7 E,80 :J
15. :UNKNOWN 3=.·31 350 :J
I E,. :UNKNOWN 33. 16 381) :J
I 7. , :UNKNOWN 35. 12 650 :J
f"ORM I SV-TIC l /87 Re·
000811
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
S.EMI'.'OL.!.TIL.'.:: OF·1:.,:..NI(~ A~J.;LYS:s o,.:.:r. SHEET _EPA ~M~F:_~ \IC.
T~NT~TIVELY IDE~~T!FIED 1:.□MPOU~JDS
Samo le 1.1t / v,:, l : t.g/ml) ~
Levl?l: < l ,: ..... ·/med) LOW
~: M,:,istLn··e: not de·:. ::·3 de,:.
<Y.'N) I'{__ 4.7
C OMF'OUND IJAME
!. ; MLI FHAT iC COMF'OUND -. : ALIF'H,\TIC HYDF'OCAF·B□N
3. l -= ~..: - -_;_ F ENTiA!NOt~E, -4 ! IYEF.OXY
4. :ALIF"HATIC HYDPOCAP80N s. : ALIF'HAT IC HY□F·ou,F:BON
E,. : UfJf:NOWfl
~ : 1•.ETONE
:3. :1:ETONE
':'. :UNl:'NOWN
l O. 1054·1-5()-t):SULFUR, MOL. (SB,
SD(j
Lab File ID:
0;1te F'1?1:ei ved:
Date E~tra~ted: <)7/02/'30
Di 1 ut i ,:,n Fa,: ::,:,r: 1. 1)0 ~--=--
CONCENTPATION UNITS:
1·ur;/L ,:,r 1.1g/h;) IJ(j/~."13
PT EST. CONC.'
3. '3:2 4:::oo
4. I ::: 21:i,:i
4 t1CT I ... 55 ~7000
4.78 320
..1. ·33 :::71)
5. '?(J 580
E,. E,7 1 '3(H)
E,. 87 €,(H)
7 • E,I) 8:20
-.:::::. 7(1 lE,(l(J
:J
: J
; E ._· -
:8J
:s..:
:BJ
:J
:J
:J
:J
----------------------------------------------------------------------
; r: y
FORM I SV-TIC 1 /87 Re·
000837
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I ,,,... ~-... ,.
I
I
SEMIVOLAT!LE OPGANICS ANALYS:S DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
_CPA S,\MP~£ NO.
S-13A-FE .:--+
:....,b rJ_;me: f:EYSTONE DJ'/.
SMS N,:,.:
t1atrix: (3011/water~ SOIL Lc.b S.;'.\mp le ID: ·;1(11)£,)081:
30.0 C:g/ml) ~ Lab File ID: 4U(lE,(H)8C::
(low/med) L~O~L~•--Date Received: 06/1)~/·30
% Moisture: n,~t de~. de•:.
(S12pF /(,:,nt /S,:,n,:) ·;on(
1::iF'C C.l eanLtD! t.Y/N) N ;,H: Dilution Factor: 1.00
C □rlCENTF:,\; I ON Ufl I TS:
! L19/L ,:,f u9li<9) U•:l/n3
C AS NUMBEF: COMPOUND NAME PT EST. CONCi
; I. :ALlF'!-iATIC COMF'OUND : 3.65 : . :::700 :~~-it:
2, 1·23 12 2··2 '"·CPlT•\PIOPlE, 1 IIVDF:8.XV METI 1.32 7-.:l?O(l :8JJ\ ';
3. : UNLNO~JN 5. 75 5€.0 : BJ
·\. : :\LJF'HAT!C COMPOUND E,. 07 330 :J
5. :VETpNE E..53 '380 ' ' . ~
F,. : IJNUJOWN ' cc . ...,..., 4(,(1 :J
7. : UNf::NOWN 8.52 .::01) :J
a. : uNn101m :::·?. 74 531) :J
9. :PHTHALATE 30. 1 :.: 2:50 :J
:i). lPHTH~LATE 3(), I 'cl 310 :J
11. : ALIPHATIC HYDF:OCAPBON 30.32 331) :J
P :ALIPHATIC HYDROCARBON 30.41 I 8() :J
13. :UNKNOWN 31. 87 2500 :J
14. : UNf,NOWN 33. :5:.:: 6:::() :J
----------------------------------------------------------------------
FORM I SV-TIC 1/87 Re
000856
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
SEMIVOLAT!LE OF·1]ANI1:S ANALYSIS DATA S}~EST _EPA SAMF·•-~ ~JC
TENT AT I '/ELY I DENT l FI ED ,: OMFOUIJDS
M ... ::..tr1:,.: 1..5,:,il/•,,1..1terJ SQIL
Sample wt/v,:,l: 30.0 fg/mL.1 §__
f l ,:,...., I ine,j) LOW
:-: M,:,isture: n,.:,t de,:. _____l_Q_ de,:.
E:·:tr.J.,:t.i,:,n: t"S:2pF/(1:•nt/S,:,n,:) SOrJi:
( y / N :, t!.._____ pH: 5.4
Lab File ID:
C O~tCENTF/1 TI ON UN 1 ;"S:
1.ug/L ,:,r-ug/kg.J Ur:J/KG
S-81)
OE,/() 1 /'30
CAS NUME:EF COMF·OIJND NAME F:T EST. CONC;
I. : ,';LJF·HAT!C COMFOUND 3.72 550 !BJ 1 -' . l_..:,-4.:... -. -f! f!l::iTnli:1O, JE 1 t ! i'1 EF.J!<Y 4 t1[f l ! . 03 03008 IL::
3. !UN/::NOWN E..05 100(1 ; 8_"
·L : ALIPHATIC COMFOIJND 5.37 ·320 :J
~ ; f ETONE E,. 30 47c) !J ~-
5. : uw·.N□tm 7.77 430 :J
'. ; AL I F·HA T I C HYDF·□,:AF·B□N :0.15 5E.O !J
8. : F·HTH,\LA TC:: :.::o. ·j·? 1600 :J
·3. !ALIPHATIC HYDF:OCAR80N 21. 34 '371) :J
10. : t\L!F'HATIC HYDROCAF'BON 22.45 77() !J
1 1 • : ALIPHATIC HYDROCARBON ::3.54 ·3E,Q :J
FORM I SV-TIC I /87 Re·
000879
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Level:
IF
SEMI '.HJL,; TI LE OF'1:0:1-\N I CS 1-\tt-'.1_ '1''= IS J1:, T,; SHEET
TENTATIVELV IDENTlF!ED (OMPOUNDS
3(>.0 (g/inl.l §___ Lab Fi le ID:
LOW Date F:e,:ei'✓ed:
i: M,:,istL1re: n,:,t de,:. de,:. Date E:,.tra,:ted:
i"Y,'N) N pH: 3. 7
(ON(ENTRATION UNITS:
1u,:;i/L ,:,r uo/:-,g.1 1)1:::n·:G
COMF·□UND NAME . EST. 1:0NC.
7.
8,
':I •
1 (l.
I I.
I.,
.. .
! urwrl □lm
: UNl:NOWN
: UrWNOlJU
: IJNl:NOWN
!UNl<NOWN
!CAPBOXYL!C
: UNl-'.NOWN
!UNKNOWN
!UNKNOWN
:t. ·:J/
:.::.c.1-. 30
:.:::5. '?6
:26.5:2
2E,.E,7
ACID :e,. '"97
27.3E.
2·':J. 76
33. E,·3
FORM I SV-TIC
511:1 :J
3:31) : _r
..;.ji) ' . ,,
..i3c) !J
510() :J
! :1)(1 :J
830 !J
1-.::(,(1 ;j
541) :J
000923
I /97 Re·
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Lz,b
IF
SE~r\JOL,-'\T!LE OF't~1\/'!I1:.s ANA:..YS:'3 D1\T:~ SHE:::i
TENT~T!','EL: IDENTIFIED 1:.C~F·OUNDS
21).0 (g/ml) §___
de,:.
CO~IPOUND Ni',ME
Lab S.3.mp 1 i·? ID:
Oat':' Fe,:r?t ·,<.?d:
1: :Jf :c::::r;,,:;_AT i. ON UN I TS:
•.ug/L ,:,r-ug/Kg) Uf:llf<r3
F:T EST. C□rJC.
: . 1. . ,_o .::.: F'E"IT,'.rJ9'<E, I l''.'CF:GX\' ! <1ET: !!i, U : . G:-:·?:· '.3_·· 1i
: '.-11\LOl:IEN.\ TED H'IDF:OC\F:8cr: E,. 5:2 1.::i:.,(, : .J :.
C,.
-1.
~ ~-
£.
7.
8.
'3.
1 (I.
I I.
I _:.
13.
14.
15.
IE,.
17. •.•
;/;'ETONE 6.97
: t:ETONE
: UIH:'NO.JN
: LJrll'}IOlm
: uw:NOWN
:ALIPHATIC COMPOUND
:UNKNOWN
: All PHAT I,: HYDPOCAF:EiQtJ
:UM'.NOWN
:uNKN□im
: All PHAT IC HY DF:OCAf<BON
:UNKNOWN
:UNKNOWN
:UNKNOWN
: UNf(NOWN
FOf.:M I SV-TIC
7. 13
7. ·;11)
8. :-:-·:~
·:t. 07
:.::.:.o:.:
:.::3. ':/()
:.::7. 3':I
30. :.:::::
31. 74
3:2. 34
32.87
3•J.01
36.4E,
::: l ('•) ! ,}
37(1 ' . ' ; :.::·:,1:,0 :J
,-i.r:,(~ : .:
430 : J
I 11)(1 : J
1300 : J
58(1 :J :so :J
31 (I : .J
1800 :J
560 :J
::so :J
·?1)0 :J
53() :J
tl0094~
1187 Re
I
I
I
I
I
I
I
I
I
I
I . ,
I
I
I
I t'.'--~':;.~ . ·• ;-_ -·: ·.:
...
I
I ........ 'I•
I
I
IF Keyst,,ne DC# 06008 -04-8
SEMIVOLATILE OPGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
_EPA SAMPLE NO ..
Lab Name: KEYSTONE ENV.
Lab Cude: KEYTX Case No. : OE,008
Matri:(: (-5,:,i l /1,,,1ater) SOIL
Sample "'t/vol: 30.0 (g/mU
Level: (! o"'/med) LOW
Y. Moisture: n,:,t dee. :20 dee.
Extra,:t ion: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) ~ pH:
Number TI Cs found: ...J2
X-46-WA
Contract: 179:80-04
SAS N,,.: SDG No.: C30WA
§__
SONC
4.5
Lab Sample ID:
Lab File IO:
Date Re,:ei ved:
Date Extracted:
Date Analyzed:
Dilution F"a,:tor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
900600819
4U06008CJS
06/06/90
06/07/90
l)E,/ 1 '3/'30
2.0
. '
CAS NUMBER COMPOUND NAME RT > ' EST. CONC •. : Q :================:=========---=-=========-----:--======:=============:====:
I. : ALIPHAT re COMPOUND 3.67 3000 :J 11 t -Q 4.: ' ' f Er4TAr40r4E, 4 ll'l'DR8XY 4 t1ET: 4.40 BJeoe ; 8.JJ!a -~ ..:.. ' ....
3. :UNKNOWN 5.92 540 J
4. :UNKNOWN 6.65 461) J
5. :UNKNOWN 7.67 72C) J
6. : ALIPHATIC COMPOUND 22.04 1100 J
7. :UNKNOWN 23.'34 :2600 J
8 . : ALIPHAT re COMPOUND 24.17 510 J
9. :UNKNOWN 28.01 350 J
I 0. :ALIPHATIC COMPOUND 28.29 510 J
11. :ALIPHATIC COMPOUND 29.97 2700 J
12. :UNKNOWN 30.27 1300 J
13. :ALIPHATIC COMPOUND 31.71 1500 J
14. :ALIPHATIC COMPOUND 31.87 790 J
15. :ESTER 32.32 930 J
16. :UNKNOWN 32.94 1600 J
17. I ALIPHATIC COMPOUND 33.54 710 J
18. :UNKNOWN 33.77 1900 ,J
' 19. -.-IUNKNOWN 35.72 740 :J ' .. .. . I ' ' -------------------------------------------' -------------------------
FORM I SV-TIC I /87 Rev
000983
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I .;~;~~
. •:t ... "' .
..
I
I .,... ,._ .. '.
I
I
IF Key st one DC• 06008 -04-e
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: KEYSTONE ENV. Contract: 179280-04
EPA SAMPLE NO.
X-7-LF
Lab C.:,de: KEYTX Case No.: 06008 SAS No.: SDG No. : C30WA
Matri:-.:: (s,:d 1 /•..1ater) SOIL
Sample 1,1t /vol : 30.0 (g/mU §.._
Level: ( I 01,1/med) LOW
'l. Moisture: not dee. _n dee.
Ext r ai: ti on: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/Nl t:!_ pH: 3.8
Number T!Cs found: _2.
CAS NUMBER COMPOUND NAME
I. :KETONE .., ~-: UNf'.NOWN
3. : ALIPHATIC COMPOUND
4. 123 .. 2 212 PEt4Tl,NO"E, 4 I IVBR □)(V
5. :UNKNOWN
6. :KETONE
7. :UNKNOWN
Lab Sample ID: 90<)60081 8
Lab File ID: 4U06008C!8A
Date Received: 06/06/90
Date E,tracted: 06/07/90
Date Analyzed: 06/26/90
Dilution F' ac t(:ir: 1.00
CONCENTRATION UN I TS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC.
3.55 230
3.93 960
4.23 1500
4 r,er 1 ... 82 62t)O0
6.07 580
6.77 200
29.64 1800
Q
lJ
:J
'J 1. ;8JA
:J I
:J
:BJ
----------------------------------------------------------------------
001013
FORM I SV-TIC l /87 Re,
I
I
I
I
I
I
I
I
I
I
I :.::. '='-;
I
I
I
I ,.-. -:_-f ~"7~-:'~
I
I ..... !'· •, •.
I
I
IF Keyst,,ne OCtl 06008 -04-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS _EPA SAMPLE NO
X-93
Lab Name: KEYSTONE ENV. Contract: 179280-04
Lab C,:,de: KEYTX Case No. : 06008 SAS No.: SOG No.: C30WA
Matri•: (soil/water) SOIL
Sample wt/v,,l: 30.0 (g/mLl G __
Level: (low/med) =L=O~W __
'l. M,,isture: not dee. _1.Q dee.
Extra,:t ion:
6PC Cleanup:
(SepF/Cont/Soncl
(Y/Nl ti__
Number T!Cs found: ~
pH: 6.3
CAS NUMBER COMPOUND NAME
Lab Sample IO:
Lab File I 0:
Date Received:
Date Extracted:
Date Analy:ed:
Dilution r a,: t QI" :
CONCENTRATION UNITS:
(ug/L or ug/Kgl UG/KG
'300600827
4U06008C27
06/07/'30
06/11/90
06/19/'30
1.00
. ' ' RT EST. CONC •. Q :================:=========-------------------:-=======:=============:=====!
I. :UNKNOWN 4.07 1800 :BJ ' ·=:. I::□ 12 212 PEPJT,'.P~OP•E, I 11\'Br:!OXY P<IETI 1. 60 I 72008 IDJ,'\ i 3. :UNKNOWN 5.'35 590 :J ~ 4. :ALIPHATIC COMPOUND 6.28 3:o :J ' 5. : ALIPHATIC HYDROCARBON 20. 15 270 :J
6. :ALIPHATIC HYDROCARBON 21.34 480 :J
7. :UNKNOWN 22.02 160 'J
8. :ALIPHATIC HYDROCARBON 22.45 400 J
'3. : ALIPHATIC HYDROCARBON 23.52 310 J
10. : ALIPHATIC HYDROCARBON 24.55 280 J
11. :UNKNOWN 2'3.82 1500 J
12. :UNKNOWN 30.8'3 310 J
13. :UNKNOWN 32.01 380 J
-----------------------------------------------------------------
001031
FORM I SV-TIC 1 /87 Re,
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I ,--~·i:"~
-. -
... -
I . '
I ......... .._ 1.
I
1•
IF Keyst,:one DCII OE.008 -04-8
SEMIVOLATILE OPGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
_EPA SAMPLE NO.
X-'34
Lab Name: KEYSTONE ENV.
Lab Code: KEYTX Case No.: OE.008
Contract: 17'3280-04
SAS No.: SDG No.: C30WA
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/ml) G __
Level: ( l ,:,w/med l LOW
I, Moisture: not dee. __ 0 dee.
E:i:tra,: ti on: (SepF/Cont/Soncl SONC
GPC Cleanup: (Y/Nl ~ pH: 5.7
Number TI Cs f,:,und: __!2
CAS NUMBER COMPOUND NAME
I. !UNKNOWN
~ : ALIPHATIC HYDROCARBON
3. :ALIPHATIC COMPOUND
L 123 12 212 POHA140P4E, I I IVBROXY
~ .,J. :UNKNOWN
E,. :ALIPHATIC HYDROCARBON
7. :ALIPHATIC HYDROCARBON
8. :ALIPHATIC HYDROCARBON
'3. :PHTHALATE
10. : ALIPHATIC HYDROCARBON
11. :ALIPHATIC HYDROCARBON
12. : ALIPHATIC HYDROCARBON
13. !ALIPHATIC HYDROCARBON
Lab Sample ID:
Lab File ID:
Date Rei: ei ved:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kgl UG/KG
-~•)OE.00828
4UOE.008C28A
06/07/'30
06/11/'30
t)6/2E./'30
1.00
RT EST. CONC, Q
=============:=====:
3.75 530 :BJ
4.02 '340 :J
4. 18
METI L75
5.'38
18.75
2000 :BJ ~ 73000 I 8.:"
720 :J
370 :J ' 1'3.'3'3 650 :J
20. 10 250 :J
20.80 1400 :J
21. 15 '360 :J
22,2'3 700 :J
24.37 630 :J
23.35 1100 :J
001055
FORM I SV-TIC 1/87 Rev
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Level:
IF
SEMIVOLATILE OPGANICS ANALYSIS DATA SHEET
TENTATIVELY !DEIITIF:ED COMPOUNDS
SMS N,:,.:
1000 (9/mL:> t!.h_ Lab File ID:
S-F' I NSA i:
4UOE.008C: ~
Date Received: 06/(t2/1()
:: Moisture: not dee. dee. Date E:~tracted: 06/04/90
('(/TJ.l ~ pH: E.O
CAS NUMBEi': ,: OMF'□UND IJAME
Diluti,~n Factor: ~l~-~O __ _
(OJ'11CENT?1\ i I ON UN I TS:
(1.19/L ,:,r 1..19/~::,;} UI~/!._
i
F:T EST. CONC;i
'----------------'--------· -------------------·--------·-------------•-----' ,-----------------,----------------------------------,----------, -·------------, -----,
!.
FORM I SV-TIC l /87 Re·
000686
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...... ,. <\1,
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IF
SEM!VOLAT!LE OPGAN!CS ANALYSIS DATA SHEET TENTATIVELY !DENT!Fl~D COMPOUNDS
SAS N,:,,:
l.QQQ_ c'g/ml> t1.b..__ Lab Fi le ID:
EPA SAMF·!..£ :00
Date Pe,:ei·,ed: i)6102/?(1
% Moisture: not dee. de(.
pH: 4.5
~Jurnber TICs found: __ I
C AS '.·!UMBEF'. COMPOUND NAME
:UNINOWN
DilL1ti,:,n Fa,:tc,r: 1.1) ~~---
,:.mJ1:en::'.1\ Tl ON UM 1 TS:
(1J9/L ,:,r ugn=:g) IJG/L.
RT EST. CONC.
I I
C
:BJ
FORM I SV-TI C 1 /87 Rev
000697
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.,,. ~-.....
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IF
SE,-1;'.'0LATILE OF·6MJI•:S i'-f·JAL',SIS D,',TA SHE!::T
TENTATl'./EL'.' ro::::r-n:rrED COMF'OJJNC'S
N,:,.:
L3b File ID:
EPA SAMF L~ ~,C.
X-F.· J NSATE
N,:,. : C30w,:.
flow/med) L=O=W __ Date Re,:eived: 1)~/<)6/·30
:~ Moisture: not dee. dee. Date E~tracted: 1)6/07/90
pH: !) i 1 u ti ,:,n Fa,: t ,:,r : 1 . 0 -'-'--"'----
,:.mK.Ei :TF:AT I ON UNITS: .
(;_19/l ,:,r ug/Kg) I.JG/I-=-!.
-~
• c,.:.,s NUMBER COMF'OUND NA~E F.·T EST. CONC. .,
I. ~4071)-77-7:cvi:L□PEtJTANOL, 2-METHYL-~ _,. 13 ::a :J
: uw.:11mJN 2£.04 : 15 : .J
3. : UNl:NOWN 2'3. 7 I ' ' ·"'.•'"'.I :E<J
000706
FORM I SV-TIC 1/87 Re
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SEMIVOLATILE OPGANICS ANALiSIS DATA SHEET
TENTATIVEI_Y iDEliTIF!~~ COMPOUNDS
~ab File ID:
(low/med) ~L~O~W~_
: Moisture: not de~. de,:.
Dil 1_1ti,:-n F::;,:t,:,r: 1.r) ~--"------
CONCENTPATION U~ilTS:
(ug/L ,:,r ug/):g) Ut'j/L
EST. CONC. '-----------------·-----------------------------·--------·-------------·-----· ,--------·-------------,----------------------. -----------, ---·-----,···------------,-----,
!. : !JNl:N □WN
: UW.NO.IN
FOF.'1'1 I SV-TIC
10.85
·:·j. 7 1
!J
:e:
000719
I /87 Re
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I ,2:"c SUPP UMENTATION
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11
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AWD Technologies, Inc.
APPENDIX C
SUPPORT DOCUMENTATION
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•
... ,_,1,.'
,: .-\S NO. ,: l)Mf·OIJIID
i:·□r-:CENTPAT I ON U~~ l .. '::
:.u;i/L ,:,,,. 1_1_9:T,:;::.• Uf~::'.J.:....
~J-87-3----------r:t1l,)r01ne~l1ane _________________ _
7+-93-·)--··------nr,,,n,,metf,.Jn,, ________________ _
73-1)1)-3---------C.~1l,)r0et~11n~------------------
·7s-(1·:;1-.::-----·----Met hy 1 ene Ch l ,:,r-.. df: __________ _
E, :--EA-t ---------.',,: at ,:,ne ______________________ _
7~-15-0---------Carbon D1sL1l fide ____________ _
75-35-4---------1, 1-Di,:hloroett,ene ___________ :
75-34-3---------1, 1-Dichl,~roett,ane ___________ :
541)-5·~-(i--------l, :.:-Oi,:hl ,:,r,:,et.hene f t,:itul ·:, ___ :
e--66-3---------(t,loroform __________________ _
10?-1:1~-:--------t,:-Dichl,)r,,ett1.1ne ___________ i
73-93-3---------~-Butanone __________________ _
71-55-€.---------1, 1, t-Tr1,:hl,:,,,.,:,c4:'.1J.n..:i _______ _
56-:3-5---------Carbon T@tract1lor1de ________ _
108-<)5-4--------Vinyl ~,:at~te ________________ :
75-:7-4---------Bromodict,loromett,ane ________ _
78-87 -5---------1 , 2-0i ,: h l ,:,r ,:,pr ,:,p,3ne __________ :
10061-01-5------cis-1,3-DicJ,loropropene ______ :
79-0l-6---------Tr1(J1l0r,,eth~n~--------------
124~48-1--------0i bromo,:h l ,:,r ,:imethane :
7~ ~~-s---------1 1 ::-Tri,:t,l,:iroet;h.J.n;;--------: ~~ ' , --------71-'-43~2---------Ben=ene _____________________ _
1 f)1)6:1 -02-6------t ran:;-l , 3-0 i ,: ht ,:,r ,:,pr ,.:,pen•:-____ :
75-25-:---------Br ,:imo f ,::,rm ____________________ :
t 08-10-1--------4-Met; hyl -~-P•::-nt .Jn,:,nQ _________ :
591-78-6--------2-Hex3n0ne ___________________ :
1-::,7-\ :3-4--------T,::it r .i,,: h l ,:i, ,:,~th· :'IC ----·-. _______ :
.-·]-34-5---------1 , 1 , :.: . 2-T1: '; r --=-•.: h: <-r ,:-,1?t han~----:
1•)8-88-3--------r,:i l uenc ------·•--·-·--__________ _
!08-90-7--------CJ,loroben:enq ________________ :
:!)0-41-4--------Eth;lb~n~en~ __________________ :
100-42-5--------Styrene _______________________ :
1330-20-7-------Xyleno (total) _______________ :
' ' ·----------------------------------------------·
FOP.MI VOA
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:u :u
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:u
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:u :u
:u :u :u
Q
I /87 Re,
000501
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• lA
VOLAT !LE OF:GAtl I CS AN,\L YS l S DATA SHEET
Key st one DC• f)E,1)08 -<.'4-,
EF'A s.,MF'L!:: 110
Lab Code: ~-EYTX Case No.: SAS N,,.: SOG No. : C31)t.J.,,
Lab Sample IO:
Sa.mp 1 e wt /v,:,l: 5. r) (g/mL) !!b....__ Lab File IO: 5Er1)605Vc):
( 1,:,\,,,1/med) LOW Date Re,:ei ved:
½ Moisture: not dee. Date Analy=ed: 06/05/'31)
C,:,l Limn: F'AO'. Dilution ~actor: 1 • t)
C,\S NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/KgJ UG/L
74-87-3---------Ct,lorometf,ane _______________ _
74-83-3---------Bromometf13ne ________________ _
75-i)l-4---------Vinyl Chloride _______________ :
75-0!J-3---------1:hlor,~ethane ________________ _
75-•:•9-2---------Methylene Chloride ___________ :
67-64-1---------Acatone _____________________ _
75-15-0---------Carbon D1sulf1de ____________ _
75-35-4---------1, l-Dichl,Jr,Jet•1ene ___________ :
75-34-3---------1, 1-Dict,Ioroethane ___________ :
541)-59-0--------1,2-Dichloroethene (total) ___ :
67-66-3---------Chloroform __________________ _
ti)?-1)6-:--------1,2-0ichloroett,ane ___________ :
78-93-3---------:-Butanone __________________ _
71-55-6---------1. 1. l-Tr1chloroethane _______ _
56-:3-5---------Carbon Tetract1lor1de ________ _
109-05-4--------Vinyl Acetate ________________ :
75-:7-4---------Bromodichloromethane ________ _
78-87-5---------1,2-0ichloropropane __________ :
l•)0E.I-01-5------c i s-1, 3-0i ch! or opr,,pene ______ :
79-01-e.---------Tr 1 ,: h I ,,r oet hene _____________ _
124"."',48-1--------Di br omoc h l or omet hane _________ :
7'3-00-:5------:---1, 1, 2-Tr i ,:h l ,::,roethane ________ :
71-43-2---------8enzene ______________________ :
10061-02-E.------t r ans-1, 3-0i ,:h I ,,ropropene ____ '
75-25-2---------Bromoform ___________________ _
108-10-1--------4-Methyl -2-Pen t an,,ne ________ _
591-78-e.--------2-Hexanone __________________ _
79-34-5---------1, 1,2,=-Tetrachloroethane ___ _
108-88-3--------Toluene _____________________ _
108-90-7--------Chl ,,r obenz ene _______________ _
100-41-4--------Ethylbenzene ________________ _
100-4::-5--------Styrene _____________________ _
1330-20-7-------Xyl ene ( t•:tt al>. ______________ _
10 ! U
10 :u
10 : U a)u
5 :u
5 :u
5 :u
~ . J :u
~ :u ~
5 :u
10 :u
~ .J :u
~ :u ~
10 :u
5 :u
~ :u ~
5 :u
5 :u
5 :u
5 :u
5 :u
5 :u
5 :u
10 :u
10 :u
5 :u
5 :u
5 :u
5 :u
5 :u
5 :u
5 :u
Q
-----------------------------------------------------------
F"ORM I VOA 1/87 Re
000508
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IA
VOLATILE OF'<:,MH CS MIAL 'ISIS DATA SHEET
Keystone DC# OE,008 -<)-I-8
EPA S'"MPLE NO.
VBL:<3
Lab 1:,~de: ~EYTX Case No.: 06008 SAS N,:,.: ____ SDG N,:i.: C-30WA
Matri:,:: (3,:,il/i..1ater) SOIL Lab Sample ID: "30061)()81)1
Sample 1.1t/vc,!: 5.0 (g/mL) §__ Lab File ID: EE<OE.OBVOI
Leve 1 : (l,:,w/med) LOU Date F:e,:cived:
'l. M,:,isture: n,:it de,:. Date Analy:ed: l)E,/08/"30
C,:,l Ltmn: (pa,:k/,:ap) PACK Diluti,:,n Fa~tor: 1. 0
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87~3---------Chloromethane _______________ _
74-83-9---------Bromometh~ne ________________ _
75-01-4---------Vinyl C•1Ioride _______________ :
75-00-J---------Chloroett,ane ________________ _
75-09-2---------Methylene Chloride ___________ :
E,7-E,4-1---------Acetone _____________________ _
75-15-0---------Carbon 01sulf1de ____________ _
75-35-4---------1, 1-0ichloroethene ___________ :
75-34-3---------1,1-Dichloroethane ___________ :
540-59-(J--------1,~-0ichloroet•1ene (total) ___ :
67-66-3---------Chloroform __________________ _
107-06-:--------1,2-0ichloroet•,ane ___________ :
79-93-3---------~-Butanone __________________ _
71-55-6---------1, 1,1-Tri~hloroett,ane ________ :
56-23-5---------Carbon Tetrachloride~--------
108-05-4--------Vinyl Acetate ________________ :
75-:7-4---------Bromodichloromethane ________ _
78-87-5---------1,2-Di~hlor,)pr1)pane __________ :
10061-01-5------cis-1,3-Dichloropropene ______ :
79-01-6---------Tr1chloroethene _____________ _
10 : U
I I) : U
10 : U )in :u
~:u
5 :u
5 :u
5 :u
5 :u
5 :u
10 : U
5 :u
5 :u
10 : U
5 :u
5 :u
5 :u
5 :u
124:,-$.8-1--------Di bromoch l •~r omet hane _________ : 5
79~-5--------1,1,2-Trichloroethane ________ : 5
:u
:u
:u
:u
:u
:u
'U
u
71"'43-2---------Benzene : 5
1ooe1-02-&------trans-1~3:otch1o~op~op~~~====: s 75-25-2---------Bromoform ____________________ : S
108-10-1--------4-Methyl-~-Pentanone _________ : 10
591-78-6--------2-Hexanone ___________________ : 10
127-18-4--------Tetrachloroett,ene ____________ : 5
7'3-34-5---------1, 1, :, 2-Tet r ac h l ,:iroethane ____ : 5
108-88-3--------Toluene ______________________ : 5
108-90-7--------Chlorobenzene ________________ : 5
100-41-4--------Ethylben:ene _________________ : 5
100-42-5--------Styrene ______________________ : S
u
u
u
u
u u 1330-20-7-------Xylene (total) _______________ : 5 : -----------------------------------------------------------
FORM I VOA
Q
1/87 Re•
00()51~
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()JG
IA Keystc.ne DC# 06008 --{,4-f
1/0L.~TIU:: OF:GAN!CS ANALYSIS DATA SHEET _EPA SAMPLE NO.
VBL~'.4
l..lb Name: t:EYS TmJE ENV.
Lab Code: rEYTX (:ase No.: 1:l6c)08 SAS N,:,.: ____ 5013 No.: C30WA
Matri:~: (3oil/~ater) WATER Lab Sampl~ ID: 90060080:
Sample .it/v,Jl: 5.0 <g/mU t!l:..__ Lab File ID: EB0609V0l
Level: LOl, Date F:e,:eived:
% Moisture: not de~. Date Analyzed: 06/09/90
(p.a,:k/,:ap) Dilution ~act,)r: _1_.r~; __ _
CONCENTRATION UNITS:
CAS NO. COMF'OUND (ug/L ,)r ug/Kg) UG/L Q
74-87-3---------Chloromethane _______________ _
74-8:-9---------Bromomethane ________________ _
75-01-4---------Vinyl Chloride _______________ :
75-00-3---------,:hloroet•iane ________________ _
75-()9-2---------Methylene Chloride ___________ :
67-64-1---------A~etone _________ · ____________ :
75-15-0---------1:arbon D1sulf1de ____________ _
75-35-4---------1, 1-Dichloroethene ___________ :
75-34-3---------1, 1-Dict,loroethane ___________ :
541)-53-1)--------1,2-Dichloroett,ene (total) ___ ;
67-66-3---------ct,loroform __________________ _
l!)7-06-2--------l,2-Dict1loroethane ___________ :
78-9J-3---------~-Butan,~ne __________________ _
71-55-6---------1, 1, 1-Trichloroett,ane ________ :
56-23-5---------Carbon Tetra~hloride _________ :
108-05-4--------Vinyl Acetate ________________ :
75-=7-4---------Bromodichloromethane ________ _
78-87-5---------1,~-Dichloropropane __________ :
10061-01-5------cis-1,3-Dichloropropene ______ :
79-01-6---------Trichloroethene ______________ :
124-48-1--------Di br omochl or,:imethane _________ :
79-00-5---------1, 1,2-Trichloroethane ________ :
71-43-2---------Benzene ______________________ :
10061-02-6------t rans-I, 3-Di ch! ,:,r,:,pr opcne ____ :
75-25-2---------Bromoform ____________________ :
108-10-1--------4-Methyl-2-Pentanone _________ :
591-78-6--------2-Hexanone ___________________ :
l :7-tS-4--------ret r ach 1,,r oethene ____________ :
79-34-5---------1, 1,2,~-Tetract,loroethane ____ :
108-88-3--------ToluQne ______________________ :
108-90-7--------Chlor<Jbenzene ________________ :
100-41-4--------Ethylbenzene _________________ :
100-42-5--------Styrene ______________________ :
1330-20-7-------Xylene (total) _______________ :
: ----------------------------------------------
FORM I VOA
.
10 ;~
10
10
3 :J
10
,U
5 :u
5 :u
~ :u _,
5 :u
5 :u
10 :u
5 :u
5 :u
10 :u
5 :u
5 :u
5 :u
5 :u
5 :u
5 :u
5 :u
5 :u
5 :u
10 :u
10 :u
5 :u
5 :u
5 :u
5 :u
~ :u _,
5 :u
5 :u
------------------
1/87
000527
Re
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IA Keystone DCI 06008 -,:4-'
VOL AT I LE OP6AN I CS ANALYSIS D1H A SHEET EPA SAMP:..~ NO.
VBLKS
Lab Mame: f.'.EYSTONE ENV. C,:,nt r .3.,: t: 1 73:80-(14
Lab C,~de: kEYTX Case No.: !)61)1)8 SAS N,:,.: ----SDG No.: C31)w,:.
M~trix: (soil/~ater) SOIL Lab S~mple ID: 90060080:
Sample 1.1t /v,,l: 5.0 /g/mU §__ Lab Fi le JD: EB0611V0l
Leve I : LOW Date Pe,:eived:
% Moisture: not dee. Date Analy:ed: 06/11/90
C,:, l umn: lpa.:k./,:ap) PACK Di 1 u ti ,:,n Fa,: t ,:;.r : 1 . 0 -'--'-"'-----
CON CENT RATION UNITS:
CAS NO. COMPOUND /ug/L or ug/Kgl UG/KG Q
74-87-3---------Ct,loromethane _______________ _ 10 :u
74-83-3---------Bromomet•iane ________________ _ 10 :u
75-<)1-4---------Vinyl Chloride _______________ : 10 :u
75-<)0-3---------Chlor,~et ►13ne ________________ _
75-0'3-::---------Met.hyl ene Ch l ,:,ride ___________ : :J
67-64-1---------Acetone _____________________ _
75-15-0---------Carbon D1sulf1de ____________ _
75-35-4---------1,1-Dichloroethene ___________ : 5 :u
75-34-3---------1~1-Dichloroethane ___________ : 5 :u
540-53-1)--------1,~-Di,:hloroethene (total) ___ : 5 :u
67-66-3---------Chloroform __________________ _ 5 :u
lt)7-()6-:--------1,2-0ic ►1loroett1ane ___________ : 5 u
78-93-3---------:-Butanone __________________ _ 10 u
71-55-6---------1, 1, !-Trichloroethane ________ : 5 u
56-:3-5---------Carbon Tetrachloride ________ _ 5 u
108-05-4--------Vinyl Acetate ________________ : 10 u
75-27-4--------·-sr omod i ch 1 or omet hane ________ _ 5 u
78-87-5---------1,2-0ichloropropane __________ : ~ .J u
10061-0!-5------cis-l,3-0ichloropropene ______ : 5 u
79-01-6---------Tr i ch l ,::,r oet hene _____________ _ 5 u
124~48-1--------Dibromochloromethane ________ _ 5 u
79.-:00-5---------1, 1, 2-Tr it.:h l oroethane ________ : 5 u
71-,-.$3-2---------Benzene 5 u
10061-02-6------trans-1, 3-Di ch L ,,ropr opene ____ :
75-25-2---------Bromoform ___________________ _
108-10-1--------4-Methyl-2-Pentanone ________ _
591-78-6--------2-Hexanone __________________ _
127-18-4--------Tetrac11loroethene ___________ _
5 u
5 ,U
10 u
10 u
5 u
79-34-5---------1,1,2,2-Tetrachloroethane ___ _
108-88-3--------Toluene _____________________ _
108-90-7--------Ch I or ,,benzene _______________ _
5 u
5 u
5 u
100-41-4--------Ethylben:ene ________________ _
100-42-5--------Styrene _____________________ _
1330-20-7-------Xylene (total> _______________ ,
'
5 ,U
5 :u
5 :u
----------------------------------------------· ------------------
FORM I VOA 1/87 Re
000538
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IA
VOLATILE OPGANICS ANALYSIS DATA SHEET
Keystone DC# 06008 --<H-!
_EPA SAMP:..E NC
VBLKE,
Lab Name: ~EYSTONE ENV. --------------
Lab (.)de: KEYTX Case No.: 1)61)<)8 SAS N,o.: ____ SDG N•o.: C30WA
Lab Sample ID: 900E,OQ80!
5.0 fg/mL) §___ Lab Fi le ID: EBOE, ! '.:VO I A
Level: Date F:e,:eived:
% Moisture: not dee. Date Analy:ed: OE,/!'.:/90
PACI( 1.0
(AS NO. •~OMF'OUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/~~13
74-87-3---------Chloromett,ane _______________ _ 11) : U
74-SJ-9---------Bromomet•i~ne ________________ _ 10 : U
75-01-4---------Vinyl Chloride _______________ : 10 :u
75-00-3---------Ctil,~roet•,ane _________________ :
75-09-2---------Methylene Chloride ___________ : :J
E,7-E,4-1---------Acetone _____________________ _
75-15-1:1---------Carbon Disulfide ____________ _ ,U
75-35-4---------1,1-Dichl,,r,Jcthene ___________ : ~ :u ...,
75-34-3---------1,1-Dichloroethane ___________ : 5 :u
540-53-l)--------t,2-Dic•1loroet>1ene (total) ___ : ~ :u ...,
67-66-3---------Chl,,roform __________________ _ 5 :u
11)7-06-~--------1,2-0ichloroett,ana ___________ : 5 :u
78-93-3---------2-Butanone ___________________ : 10 :u
71-55-6---------1,1, 1-Tri•:hloroethane ________ : 5 :u
56-=3-5---------Carbon Tetrachloride ________ _ 5 :u
108-05-4--------Vinyl Acetate ________________ : 10 :u
75-27-4---------Bromodichloromethane _________ : 5 :u
78-87-5---------1,2-Dichloropropane __________ : ~ :u ...,
10061-01-5------cis-1,3-Dichloropropene ______ : 5 :u
79-01-E,---------Trichloroethene ______________ ! 5 :u
124~8-l--------Dibromochloromethane _________ ! 5 :u
79-Q0-5---------1,1,2-Tri~hloroethane ________ : 5 :u
71-◄3-2---------Benzene _____________________ _ 5 :u
10061-0:-6------trans-1,3-Dichloropropene ___ _ 5 :u
75-25-2---------Bromoform ___________________ _ 5 :u
108-10-1--------4-Methyl-2-Pentanone ________ _ 10 :u
591~78-6--------2-Hexanone __________________ _ 10 :u
127-18-4--------Tetra1:hloroet•1ene ___________ _ 5 :u
7':1-3·t-5---------1, 1, 2, 2-Tetrachlor,:,ethane ___ _ 5 :u
109-88-3--------Toluene _____________________ _ ~ :u ...,
108-90-7--------Chlarobenzene _______________ _ s :u
100-41-4--------Ethylbenzene ________________ _ 5 :u
100-42-5--------Styrene _____________________ _ s :u
1330-20-7-------Xylene (total> ______________ _ 5 :u
-------------
FORM I VOA
Q
1/97 R,
000549
I
D
H
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• lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
Keyst<>ne DCI OE,006 -:l-'-(
EPA SAMPLE fJC
vsu:7
L3b N3mn: KEYSTONE ENV.
Lab Code: ~EYTX Case No.: OE.008 SAS No. : SDG N,,. : C30WA
Lab Sample ID: '300€,0080 I
Sample wt/v,:,l: 5.0 (g/mL) §_ Lab F"i I e ID: EBOE,14V0l
L<?vel : ( I ,:,•.;/med) LO~J Date Re,:ei •,1ed:
% Moisture: not dee. Date Analyaed: <)E,/14/90
C,:,l umn: f p,3,: k / ,: ap) PACK Dilution ra~t,~r: 1.0
COMF'OUND
CONCENTRATION UN ITS:
<ug/L ,:ir ug/Kg) UG/KG
74-87-3---------Ct,loromethane ________________ :
74-83-3---------Bromomett,~ne __________________ :
75-01-4---------Vinyl Chloride _______________ :
75-00-3---------i::h l ,:,r ,.:,et h.::1.ne _________________ :
75-09-2---------Mettiylene Ct,loride ___________ :
67-64-1---------A~et,)ne _____________________ _
75-15-0---------Carbon Disulfide _____________ :
75-35-4---------1, 1-Di~►,l•~roethene ___________ :
75-34-3---------1,1-Dichloroethane ___________ :
540-5·~-<)--------1,:-0i~►1loroet•1ene ttotal) ___ :
67-66-3---------Chloroform ___________________ :
1(17-06-:--------1,:-Dic ►,l,)roethane ___________ :
78-93-3---------:-Butanone ___________________ :
71-55-6---------1,t,1-Tri,:•1loroet ►1ane ________ :
56-:3-5---------Carbon Tetrachloride _________ :
108-05-4--------Vinyl Acetate ________________ :
75-27-4---------Bromodichloromethane _________ :
78-87-5---------1, :-Di ,:h l •:ir,:,propane __________ :
10061-01-~------cis-1,3-Dichloropr<>pene ______ :
79-01-6---------Trichloroethene ______________ :
124:-<18-1--------Dibr<>mochlorometliane _________ :
79-Q0-~---------1, 1, 2-Tr i ,: h 1 ,Jr ,:,ethane ________ :
71-.43-2---------Ben: ene ______________________ :
10061-02-6------t r ans-1, 3-Di ch l or,:,pr opene ____ : 75-25-2---------Bromoform ____________________ :
106-10-1--------4-Methyl-2-Pentanone _________ :
591-78-6--------2-He .x anone ___________________ :
1:7-18-4--------Tetrac•11oroethene ____________ ,
79-34-5---------1,1,2,2-Tetrachloroethane ___ _ 108-98-3--------Taluane _____________________ _
106-90-7--------Clil<>robenaene _______________ _
100-41-4--------Ethylbenzene ________________ _
100-4:-5--------Styrene _____________________ _
1330-20-7-------Xylene (total) ______________ _
10 :u
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10 :u
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5 :u
5 :u
10 :u
5 :u
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5 :u
5 :u
5 :u
5 :u
5 :u
10 :u
10 :u
5 :u
5 :u
5 :u
5 :u
5 :u
5 :u
5 :u
-----------------------------------------------------------
F"ORM I VOA
Q
1/67
000559
Re
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P(JC,
IA
')OLAT!LE OF:GAN!CS ANALYSIS DATA SHEET
fCeystone DCI 06008 -,_"\4-;
_EPA 5AHPL£ NC.
'JBU'.8
Lab Code: KEYTX Case No.: 06008 SAS N,o,: ____ 5013 No.: C30WA
M3tri~: <soil/water) WATEP Lab Sample ID: 90060080~
Sample \Jt/v,ol; 5.0 (g/mU t!b_ Lab Fi le ID: 6B061-IVOI
l_evel: ( l ,:,w/med) LOl" D.>ta Re,:ei·,ed:
% Moisture: not dee. Date Analy:ed: 06/14/3<)
PACK Dilution Factor: l • 0
CAS NO. COMPOUND
CONCENTRATION UN ITS:
( ug/L cir ug/Kg) U13/L
74-87-3---------CJ,lorometJ,ane _______________ _ 10
7t-8J-9---------Br,,momethane ________________ _ 10
75-i)l-4---------Vinyl Chloride _______________ : 10
75-00-3---------~J,l,~roet•iane ________________ _ 10
75-09-:---------Metf,ylene Chloride ___________ :
67-64-1---------A~etone _____________________ _
75-15-0---------Carbon D1sulf1de ____________ _ cl)
J
75-35-4---------1,1-Dict,l~roethene ___________ : 5
75-34-3---------1, 1-Di~hloroethane ___________ : 5
540-59-1)--------1,2-Di,:•itor,)ett,ene (tot~l) ___ : 5
67-66-3---------Chloroform __________________ _ 5
107-06-:---~----1,~-Di~hl,,r,,ett,~ne ___________ : 5
78-93-3---------:-Butanone __________________ _ 10
71-55-6---------1, 1, 1-Tri~hloroett,ane ________ : ~ J
56-~3-5---------Carbon Tetrachloride ________ _ 5
108-i)S-4--------Vinyl Acetate ________________ : 10
75-~7-4---------Bromodichloromethane ________ _ 5
78-87-5---------1,:-Dichloropropane _________ _ 5
10061-1)1-5------c i s-1, 3-Di chi oropropene _____ _ 5
7'3-01-6---------Trir.hloroethene _____________ _ 5
124-48-1--------Di bromoch 1,::iromethane ________ _ 5
7'3-Q0-5---------1, 1, 2-Tr i r. hi or,oethana _______ _ 5
71-43-2---------Benzene _____________________ _ 5
10061-02-6------t rans-I, 3-Di chi or,,pr-,pene ___ _ 5
75-25-2---------Bromoform ___________________ _ 5
108-10-1--------4-Hethyl-2-Pentan-,ne ________ _ 10
591-78-6--------2-Hexanone __________________ _ 10
127-18-4--------Tetrachloroethene ____________ • 5
79-34-5---------1, 1,2,2-Tetrachloroethane ____ : 5
108-88-3--------Toluene ______________________ : 5
108-90-7--------Chlorobenzene ________________ : 5
100-41-4--------Ethylbenzene _________________ : 5
100-42-5--------Styrene ______________________ : 5
1330-20-7-------Xylene (total) _______________ : 5
-------------
FORM I VOA
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Q
1/87
000568
Re·
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IA Keystone OCII OE,01)8 -C-1-:
EPA SAMPL!a NO
'J8U('3
L~b Name: ~EYSTONE ENV.
Lab C,:,de: t:EYTX Case N,:,. : (JE,()08 SAS N,:,.: ____ 50'3 No.: C30WA
Lab Sample 10: 50060080:
Sample wt/v,:,l: 5.0 (g/ml) t!.b._ Lab File ID: EB•)6 I 5VO I
Level: llow/med) L=O~W __ Date Re,:ei ved:
~~ Moisture: not dee. Date Analy:ed: 06/15/90
(,:,1 uinn: Dilution ~a~tor: t. 0
CAS NO. COMF'OUMD
CONCENTF:A TI ON UN ITS:
(ug/L or ug/•(g) UG/L
74-87-3---------c,,loromethane _______________ _
74-83-9---------Brom,)mothan•~-----------------75-01-4---------Vinyl Chloride _______________ :
10 : t;I
10 :u
IO : \j
75-1)1)-3---------c,,1orc,eth3ne ________________ _
75-09-:---------Methylene c,,1oride ___________ :
67-64-1---------Acetone _____________________ _
75-15-0---------Carbon 01sulf1de ____________ _ GP:
75-35-4---------1, 1-0ichl,)rocthen~ ___________ : 5 :u
75-34-3---------1, 1-Dichloroethane ___________ : ~ :u ..,
540-59-0--------1,:-0i,:hl1)r,)ethene (total) ___ : ::: :u
67-66-3---------Chloroform __________________ _ 5 :u
107-06-:--------t,~-01c•,1or0et•1ane __________ _ ::: :u
79-93-3---------:-Butanone __________________ _ 10 :u
71-55-6---------1, l, l-Tri,:hl 1lroet•1ane ________ : 5 :u
56-23-5---------Carbon Tetrachloride ________ _ ~ :u ..,
108-05-4--------Vinyl Acetate ________________ : 10 :u
75-27-4---------Bromodi.: hl ,:,romet hane ________ _ 5 :u
78-87-5---------1,~-0ichloropropane _________ _ 5 :u
1ooe.1-01-5------cis-1,3-0ichloropropene _____ _ 5 :u
79-01-6---------Trichloroethene _____________ _ 5 :u
l 24;c48-1--------0i br omoc h I or ,:,methane ________ _
79~-5---------1, 1, :?-Tri ch I or ,,ethane _______ _
71-"43-2---------Benzene
10061-02-e.------trans-1~3:oi~hto~op~ope~e::::
5 :u
5 :u
5 :u
5 :u
75-25-2---------Bromoform ___________________ _ 5 :u
108-10-1--------4-Methyl-:-Rentanone ________ _ 10 :u
591-78-6--------:-He•anone __________________ _ 10 :u
127-18-4--------Tetrdchloroethcne ___________ _ 5 :u
7'3-34-5---------1, 1, 2, 2-Tet r a,:h l ,::,r,:,ethane ___ _ 5 :u
108-88-3--------Toluene _____________________ _
108-90-7--------Ch I or ,:,benzene _______________ _
5 :u
5 :u
100-41-4--------Ethylbenzene ________________ _
100-42-5--------Styrene _____________________ _
1330-20-7-------Xylene <total) ______________ _
5 :u
5 :u
5 :u
• • ·----------------------------------------------' -------------
FORM I VOA
Q
1/87 Re
000576
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lC
SEM l 1,0L.~ T ! LE 1JF:1:,,v1 r ,:·s 1\N1\L 'IS l S D1\ T ,\ SHEET
Keyst,,ne DC# 06008 -04-
EPA SAMF:_E NC
Lab rlame: KEYSTONE ENV.
Case N,:,. : OE..008 SAS N,:,.: soi:; N,:,.: (:3(lWA
/"':.1tr: .. ;: (·,:;,:.~1/•..Jctter:i SOIL L.>b Sample ID: 50(Jr:,(H)80!
Lab File ID: 4B06008CO'.::
Date Re,:eived:
% Moisture: not dee. de,:. Date E.-..;tra,:ted: (iE,/(17 /'3•)
GPC Cle;\nup: (_Y/N) ~ pH: 6.0 Di 1 ut i ,:in fa,:t,::,r: 1. Of)
'
COMF:OUND
1:0NCENTF:ATION UNITS:
(L19/L ,:,r ug/L'g) UGn:::,,;
93-<)"3-:---------3-Nitroaniline ______________ _ IE.00
83-3:-3---------A~ehapt,t!,ene _________________ : 330
51-:8-5---------:,4-Dinitrop!ienol ____________ : 1600 101J-0:-7--------4-Nitropt1enol ________________ : 1600 13:-64-3--------Dibenzofuran _________________ : 330
1:1-14-:--------2,4-Dinitrotoluene ___________ : 330
84-66-:---------Diethylphthalate _____________ : 330
70()5-7:-3-------4-Chlorop•1enyl-p•1enylether ___ : 330 86-73-7---------Fluorene ____________________ _ 331)
100-10-6--------4-N1troan1!1ne ______________ _ 1600
534-52-1--------4,6-0initro-2-Met•iylphenol ___ : 1 E,(Jc)
86-30-6---------N-Nitrosodiohenylamine lll ___ : 331)
101-55-3--------4-Brom,,p>,enyl-phenylether ___ _ 330
118-74-1--------Hexachlorobenzene ___________ _ 330
87-86-5---------Pentachlorophenol ___________ _ 1600 85-01-8---------Phenanthrene ________________ _ 330
120-1~-7--------Anthracene __________________ _ 330
84-74-2---------Di-n-Butylphthalate _________ _ 330
206'-44-0--------Fl uor ant hene
1 29.--~0-0--------Pyr ene _____ -= ================ 85-68-7---------Butylben:ylphth.:ilate ________ _
91:;94-1---------3, 3' -Di,: h I or obenz i dine ______ _
331)
330
330
660
56-55-3---------Benzo(a)Anthracene __________ _ 330
218-01-9--------Chrysene ____________________ _
117-Bl-7--------bis(2-EthylhexyllPhthalate __ _
117-84-0--------Di-n-Octyl Phthalate ________ _
205-99-2--------Benzo(b)Fluoranthen~---------331)
::o?-CS-·3--------Ben= ,:i ( ~ J F"l u,:,r anthene ________ _ 330 50-32-8---------Ben=o(alPyrane ______________ _ 330
133-23-5--------Indeno(l,~,3-cdlPyrene ______ _ 331)
53-70-3---------Dibenz(a,}1)Anthracene _______ _ 331)
191-24-2--------Benzo(g,h,i)Perylene ________ _ 330
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FORM I SV-2 1 /87 Pe,
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1C
SEMIVOLAT!LE OF\jANICS ANALYSIS DATA SHEET
Keyst,,ne DCtt 06008 -04-
_EPA SAMPLE NC
SBLK5
Ldb Name: KEYSTONE ENV. C,:,n tr a,: t : 1 7·:r:'.8(1-04
Lab (,:,de: f•:EYTX Case N,:,. : 060()8 SAS N,,.:
Matr i :,. : (s,:,i 1 /1..1ater) WATEF: Lab Sample ID: ':'(l(JE,(H)81):
Sample 1,,,1t /v,:.l: 1000 (g/mU t!h...._ Lab File ID: 480504Cr):
Level: (l,:,1,,,1/med) LOW Date F.'e,: ei ved:
'l. M,:,i sture: not dee. de,:. Date E.-..:tra,:ted: OE, I 1)4 / '30
£-,_ tra,: ti ,:,n: (SepF"' /C,:mt /S,:,nc) CONT Date Analy:ed: 06/:'c)/9()
GF'C Cle-1nup: <YIN) t:,!_ pH: £.0 Di Iuti,,n F"a,:t,:,r: I.!)
CAS NO. COMPOUND
CONCENTPATION UNITS:
!ug/L or ug/KgJ UG/L
93-03-2---------3-Nitroaniline ______________ _
83-3:-9---------Acenaphthene _________________ :
51-:8-5---------2,4-Dinitr,)pt,enol ____________ t
100-0:-7--------4-Nitropfienol ________________ :
132-64-9--------0iben:ofuran ________________ _
121-14-:--------2,4-Dinitrotoluene ___________ :
84-£6-2---------Diethylphthalate _____________ :
7005-7:-3-------4-Chlorophenyl-phenylett,er ___ :
86-73-7---------Fluorene ____________________ _
100-10-5--------4-Nitroaniline ______________ _
534-5:-1--------4,6-Dinitro-2-Methylp ►ienol ___ :
8£-30-E,---------N-Nitrosodipheny!amine 11) ___ :
101-55-3--------4-Bramopheny!-phenylether ____ :
118-74-1--------He,ach!orobenzene ___________ _
87-86-5---------Pentachlorophenol ____________ :
85-01-8---------Phenanthrene ________________ _
120-12-7--------Anthracene __________________ _
84-74-2---------Di-n-Buty!phthalate _________ _
206-44-0--------Fluaranthene ________________ _
129-00-0--------Pyrene ______________________ _
85-68-7---------Butylbenzylphthalate ________ _
'31-94-1---------3, 3' -Di,: hl oroben.: i dine ______ _
56-55-3---------Benzo(a)Anthrdcene __________ _
218-01-9--------Chrysene ____________________ _
117-81-7--------bisl2-Ethylhexyl1Phthalate __ _
117-84-0--------Di-n-Octyl Phthalate ________ _
205-99-2--------Benza(b)Fluoranthene ________ _
207-08-9--------Benzolk)F!uoranthene ________ _
50-3:-e---------Ben:o(a)Pyrene ______________ _
193-39-5--------lndenoll,2,3-cd)Pyrene ______ _
53-70-3---------Dibenz(a,h)Anthracene _______ _
191-24-2--------Benzolg,h,i)Perylene ________ _
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----------------------------------------------------------------(1) -Cannot be separated from Oiphenylamine 001335
FORM I SV-2 I /87 Re,
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6A Keystone DC# 06008 -04-17
VOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: KEYSTONE ENV. Contract: 179280-04
SAS No.: Lab c,,de: KEYTX Case No.: 06008 so,; No. : C30WA
InstrLtment ID: 5=!E~F'-----Calibrati,,n Date(s): 06/05/90 06/05/90
Matrix: rsoil/waterl WATER Level:llow/medlL __ o-w __ Column: !pa,:k/,:.3p) PACK
Min RRF for SPCC(#) = 0.300 (0.250 for Bromoform) Max ¼RSD for CCC(*) = 30.0%
:LAB FILE 10: RRF20 = SS060SV03 RRFSO-=-SS060SV02A _____ _
: RF:F I 00= 5S0605V04 RRF I SO= SS0605VOS RRF200= 5S060SV06A
' '---------------------------------------------------------------------: : : :
1:□MPOUND :RRF20 :RRF50 RRFIOO:RRF150:RRF200: RRF PSD :
,'Ch! or ,:,methane ______________ # O. 853: 0.931 0. 944: 0. 93€.: O. 922: O. 917 4. 0#
:Bromomethane _______________ 0.601: 0.558 0.772: 0.623l 0.629: 0.637 1:.1:
:Vinyl Chloride _____________ * 0.714: 0.548 0.02s: 0.744: 0.421: 0.650: :-::;.1*
:Chloroethane _______________ 0.484: 0.480 0.508: o.s10: 0.443: 0.485: 5.6:
:Methylene Chloride _________ : 0.985: 0.976 0.774: 0.894: 0.904: 0.907cI' ."3:'
:A,:et,:ine ____________________ 0.842: 0.406 0.238: 0.200: 0.201: 0.3n• 72.5:
:Carbon D1 sulfide___________ 1. 606: 1. 817 1. 446: 1. 523: 1. 727' 1. 624 :: :
:1,1-Di•:hloroethene _________ ,. 0.'349: 1.010, 0.730: 0.974! 0.739 0.880: 15.3+
:1,1-Dichloroethane _________ # 2.381: 2.399: 2.425: 2.459: 2.405 2.41~: !.2#
:1,2-Dichloroethene (t,,tal)_: L126 1.163: 1.142: 1.151: 1.1'36 1.156: ::!.3:
,'Chl,:,roform _________________ * 2.133 2.182: 2.193: 2.230: 2.230 2.194a' 1 8.L.
]1,2-Di,:hloroethane _________ 1.:::·33 1.252: 1.199: 1.227: 1.269 1.24.8: ~.9:
:2-Butanone _________________ O. 1'36 o. 125: 0.088: 0.091: 0.100 0.120 37.4:
: 1, I, I-Trichloroethane______ 0.371 0.381 0.373: 0.374: 0.373 0.374l--LO:
:Carbon Tetrachloride _______ 0.304 0.319 0.316! 0.318: 0.321 0.316 2.1:
:Vinyl Acetate ______________ 0.902 0.794 0.741: 0.744' 0.731 0.782 9.1:
:Bromodichloromethane _______ 0.524' 0.540 0.546' 0.549 0.540 0.540 1.B:
:1,2-Dichloropropane ________ * 0.426 0.435 0.437 0.439 0.433 0.434 1.2+
:cis-1,3-Dichloropropene ____ : 0.571 0.592 0.605 0.610 0.599 0.595 2.6:
:Tr1chloroethene ____________ 0.399 0.411 0.398 0.3'31 0.393 0.398 :.o:
!Oibromochloromethane _______ 0.454 0.453 0.444 0.442 0.432 0.445 :.o:
: 1, 1,2-Trichloroethane ______ : 0.403 0.369 0.347 0.342, 0.329 0.358 8.1:
:Benzene ____________________ 0.841 0.869 0.875 0.854: 0.828: O.B53 2.3:
:trans-1,3-Dichloropropene __ : 0.249 0.261 0.268 0.210: 0.263: 0.262 3.1:
:Bromoform __________________ # 0.355 0.328 0.299 0.3041 0.304: 0.318 7.4#
'4-Methyl-2-Pentanone _______ : 0.739 0.550 0.420, 0.420: 0.474: 0.5211 25.6:
2-Hexanone ________________ 0.553 0.387 0.3001 0.3021 0.335: 0.375: 28.1:
Tetrachloroethene __________ : 0.4131 0.420 0.4061 0.3901 0.409: 0.408: 2.7:
I, 1,2,2-Tatr.chloroethane __ # 1.064: 0.843 0.7161 0.704: 0.701: 0.806: 19.4#
Toluene ____________________ * 0.614: 0.643 0.6401 0.6351 0.669: 0.640: 3.1+
Chlorobenzene ______________ # 0.870: 0.896: 0.899: 0.8801 0.8971 0.888: 1.4#
Ethylbenzene _______________ * 0.349: 0.3771 0.379: 0.371: 0.389: 0.3731 4.0+
Styrene ____________________ : 0.7001 0.732: 0.740: 0.7331 0.7771 0.7361 3.7:
Xylene (total) _____________ : 0.394: 0.405: 0.410: 0.411l 0.445: 0.413: 4.6:
======================================================c=================:
Toluene-de _________________ : 1.041: 1.0451 1.0591 1.0681 1.1031 1.063: 2.3:
Bromofluorobenzene : 0.7031 0.7101 0.7211 0.7341 0.766: 0.727: 3.4:
f,2-Dichloroethane-d4 ______ : 1.289: 1.219: 1.171: 1.20s: 1.269: 1.231: J.9:
I I I I I I I
---------------------------·------·------·------·------'------'------·---FORM VI VOA 1/87 Rev
000380
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I •
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I .5~
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I
I . .,. ,-,._
I
I
I
E.A K•yston• DC• 06008 -0-4-17
VOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: KEYSTONE ENV.
Lab C,:,de: KEYTX Case No. : 06008
C,,n tract : 17'3::::80-04
SAS No.: SDG No.: C30WA
Instrument ID: =5~!~E~F __ _ Calibration Date(s): 06/04/90 06/04/90
Matri,:(soil/waterl WATEP Level:(low/medl LOW Column: lpack/capl PACK
Min RPF for SPCCt#) = 0.300 (c).250 for Bromoform) Ma~ %RSD for CCC(+) = 30.0X
:LAB FILE 10: RRF::::o = 550604V03 RRF50 = 5SOE.04V02A _____ _
:RRF!OO= 550604V04 RRFl50= 550604V05 RRF::::OO= 5SOE.04V06
' '---------------------------------------------------------------------
: : : : : : I
COMPOUND : RRF20 : RRF50 : RRF I 00: RRFI 50: RRF200: RRF : RSO :
:--------------·-------------:------:------:------:------:--==-=:--=---:-----:
:Chloromethane ______________ # 0.643 0.569: 0.615:
:eromomethane _______________ 0.598 0.430: O.G22:
:vinyl Chloride _____________ * 0.557 0.425: 0.596:
:chloroethane _______________ : 0.399 0.360: 0.421!
:Methylene Chloride _________ : 0.855 0.728: 0.644:
:Acetone ____________________ 0.506 0.306: 0.209'
:carbon Disulfide ___________ 1.167 1.467: 1.164
:1,1-0ichloroethene _________ * 0.414 0.413: 0.304
:1,1-0ichloroethane _________ # 2.246 2.302: 2.267
:1,2-Dichloroethene (t,:,tall_: 1.080 1.169: 1.103
:chloroform _________________ * 2.064: 2.170: 2.095
: 1, :-Diehl ,:,.,,:,ethane _________ : 1. 184: 1. :2::2: 1. 139
:2-Butanone _________________ 0.166: 0.125: 0.094
:t,1,1-Trichloroethane ______ : 0.354: 0.390: 0.371
:carbon Tetrachloride _______ 0.297: 0.3381 0.321
:vinyl Acetate ______________ : 0.812: 0.7811 0.759
:sromod,chlorometha~e _______ 0.491: 0.541: 0.535
: 1,2-Dichloropropane ________ • 0.335: 0.421' 0.417
:,:is-1,3-Dichloropropene ____ : 0.522: 1).580 0.579
:Tr1chloroethene ____________ 0.387: 0,426 0.404
:Oibromochloromethane _______ : 0.4381 0.473 0.455
:1,1,2-Trichloroethane ______ : 0.373 0.374 0.354
:Benzene ____________________ 0.786 0.855 0.845
:trans-1,3-Dichloropropene __ : 0.230 0.258 0.256
:sromoform __________________ # 0.348 0.365, 0.338
:4-Methyl-2-Pentanon• _______ : 0.644 0.536: 0.444
'2-Hexanone ________________ : 0.464 0.3731 0.316
Tetrachloroethene __________ 0.399 0.444' 0.418
1,1,2,2-Tetrachloroethane __ # 0.941: 0.858 0.752
Toluene ____________________ * 0.587: 0.664 0.640
Chlorobenzene ______________ # 0.8431 0.952 0.913
Ethylbenzene _______________ • 0.355: 0.426 0.4031
,Styrene ____________________ : 0.760: 0.868 0,8421
!Xylene (total> _____________ : 0.4551 0.505 0.4831
o.556:
0.473:
0.4371
o. 371:
o. 701 :
0.179:
1.318
0.336
2.262
I. 121
2. 106
I. 158
0.08'3,
0.367
0.321
0.718
0.526
0.411
0.574
0.3'35
0.449
0.337
0.809
0,253
0.33:5
0.429
0.299'
0.412
0.722
0.645
0.894
0.400
0.833
0.481
0.12s:
o.510:
0.4321
0.394'
0.687
o. 137
1. 248
0.384
2.240
I. 132
2.083
I • 158:
0.079
0.359
0.317
0.6'34
0.51S
0.403
o.558
0.388,
0.438'
0.323
0.793
0.248
0.327
0,417
0.271
0.404'
0.694
0.637
0.878
0.398
0.821
0.482
(). 622'
0.528
0.501
0.389
0.723
0.267
1. 27;3
0.3701
2.263:
I. 121:
2. 104:
1. 11:::
0. II I I
0.368:
0.319:
0.753:
0.522:
0.4091
0.5b3:
0.400:
0.451:
0.352:
0.818'
0.249
0.343
0.494
0.345
0.41:5
0.793
0.6351
0.8961
0.3961
0.825/
o. 481:
10.9#
15. 4:
15.0•
6.2:
13. Z+
I. I#
3.0:
I. '3*
2.7:
31. '3:
3.8:
4.6:
6.3:
3.8:
2.6•
4.3:
4.0:
3.2:
6.3:
3.8:
4.5:
4. 311
19.4:
22. 2 !
4. 2:
13.0#
4.5•
4. 511
6.5•
4.9
3.7
:================= .=========================================================
:Toluene-dB _________________ 0.962: 1.010: 1.0511 1.0381 1.007: 1.0141 3.4
:Bromofluorobenzene : 0.740: 0.757: 0.8071 0.790: 0.756: 0.770: 3.6
: !,2-Dichloroethane-d4 ______ : I. 146: I. 1601 1. 1251 1.131/ 1.0971 1. 1321 2.1
' ' . ' ' '
FORM VI VOA 1/87 Rev
000354
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I
I
!P<-
6A Keystone DC# 06008 "-04-17
VOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: KEYSTONE ENV, Contract: 179280-04
Lab Code: KEYTX Case No,: 06008 SAS No.: SOG No, : C30WA
Calibration Date(s): 06/07/90 06/07/90 Instrument 10: 4~0~0~0~--
Matrix: (soil/water) SOIL Level:(low/med)L ==O~W __ Column:(pack/cap) PACK
Min RRF for SPCC(#) = 0.300 (0,250 for Bromoform) Max ¾RSO for CCC(*) = 30.0%
:LAB FILE IO: RRF20 = ES0607V03 RRF50 = ES0607V02A -----
:RRFIOO= ES0607V04 RRF150= ES0607V05 .RRF200= ES0607V06
1--JJ ( (l---0
)
:===========================:======:====== ======:======
COMPOUND IRRF20 lRRF50 RRF1001RRF150 RRF200l RRF" : RSD :
' ' '
!-/o('> -.../ :Chloromethane _______ · ______ # 0,520: 0.580 0,569: 0.555
I' <? lBromomethane : 0,732: 0,872 0,718 0.784
(
') ~1)/):Vinyl Chloride _____________ * 0,934 0.975 0.964 0.966 ~(/ (7-, :Chloroethane _______________ : 0.514 0.560 0.528 0,515
1 · ~ :Methylene Chloride _________ : 1.286 1.124, 1.011 0.993 / '3 l O-%/) :Acetone ____________________ 0.689 0.409 0.302 0.218
(,
~) :carbon Oisul fide ___________ 2,307 2.603 2.327 2.383 ("_,/] J-: I, 1-Dichlor,oethene _________ * 1.120 I. 185 1.070 1.066'
I 2C.-(fJ-1--) :t,1-0ichloroethane _________ # 1.962 2.111 1 976 1.993
-~7 :1,2-Di,:hloroethene (total)_: 1.152 1.266 1:162 1.167
:Chloroform _________________ * 2.809 3.033 2.759 2.776
:t,2-0ichloroethane _________ : 1.872 1.877, 1.728 1.725
I : 2-Butanone_________________ 0. 134 0. 116.: 0. 110 0. 091
:1,1, I-Trichloroethane ______ : 0.846 0.829 0.781 0.811
'f ..,,, Jfb :carbon Tetrachloride _______ 0.908 0.837 0.873 0.903
:Vinyl Acetate ______________ : 0,453 0.357 0.359, 0.352 t . 7 ·. :Bromodichloromethane 0.834 0.813 o. 776: 0.800
_, _· -~ : 1,2-Dichloropropane_=======* _0.328 0.322 0.316: 0.329
/1''-:cis-1,3-0ichloropropene ____ : 0.705 0.700 0.677: 0.694
:Trichloroethene : 0.480 0.483 0.456: 0.456 1_93 /, _\:Oibromochloromethane _______ : 0,838 0.750 0.705: 0.702
. $JIII0~-..,.1,1,2-Trichloroethane ______ : 0.409 0.338 0.326: 0.321
1/-0 'Benzene : 0,823 0. 791 O. 754: 0. 766 aJA trans-1;3:01chloropropene==: o.363 o.346 o.339: o.343 --71/J Bromoform __________________ # 0.747: 0.655 0.617: 0.608
. 4-Methyl-2-Pentanone _______ : 0.299l 0.220 0.202: 0.180
2-Hexanone _______________ 0.257: 0.245 0.198: 0.161
Tetrachloroathene _________ 0.509: 0.636, 0.477: 0.461
1,1,2,2-~■trachloroethane __ # 0.8651 o.764: 0.618: 0.585
Toluene __ · ________________ * 0.670: O. 726: 0.629: 0.618 I
,Chlorobenzene ______________ # 0.923: 1.021: 0.899: 0.896
:Ethylbenzene _______________ * 0.424l 0.522l 0,438l 0.420
:Styrene __________________ 0.8691 1.0801 0.918l 0.856
lXylene Ctotall _____________ : 0.534l 0.6271 0.524l 0.513
-.------,-----, o.558: o.556:
0.716: 0.764:
0.937: 0.955:
0.530:
1 • 006:
0.133:
2.327:
1.0321
1.891:
1. 109:
2.618:
1.618:
0.062:
0.722'
0.714
0.318
0.727
0,305
0.642
0.434
0.650
0.304
0.738
0.321
0.554
0.156
0.114,
0.433:
0.512:
0.579l
0.838:
0.529: 3.5:
1.084: 1M:
O. 3:30: (61._5:
2. 389 : '-----5:' 1 :
O. 391 I
0.7991
1. 0'95:
1. 987:
1.171:
2.799:
1. 7EA:
0.103:
0.798:
0,847:
0.368:
0.790:
0.320:
0.684:
0.462:
0.729:
0.340:
0.774
0.342
0.636 o. 211 o. 195
0.503
0.669
0.644
0.915,
0.439:
0.9041
0.4861 0.5371
5.4•
4,011
4.9:
S.4•
6.2:
26.6:
6. 1 :
9.4:
13.7:
s.2:
3. 1 •
3.7:
4.4:
9.7:
12.0:
4.3:
4.4:
11. 3#
25.8:
30.4:
15.7'
21.41
8. 7•
7.34
11. 3,
11.8
10.0
I
I
I
I
:Toluene-dB _________________ 1.l39l 1.0541 1.024l 1.0031 0,966: 1.0371 6.3
18romofluorobenzene l 0.877l 0.780: 0.742l 0.8231 0.7251 0.7891 7.8
l'l,2-0ichloroethane-d4 ______ : 1.8831 l.696l l.645l 1.6271 1.5741 1.685: 7.1
---------------------------------------------______ I ______ -----------FORM VI VOA _l/87 Re
000328
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
1)€,<)08 -:•➔-:
VOLATILE OF·,:;ANICS INITIAL CALIE<F'ATION DATA
L~b Nama: ~EYSTONE ENV. C.:,nt r a,: t:
Lab ,: ,:,de: f:EYT :< SD(j No. : C30w;.
Instrument ID: 4~· •~)~0~0:._ __ C..llibrati,:,n Date('!i): 05/31/":fO
Matri~: (soil/water) WATER Level: (·low/med) L.O~W~-C.:,lLtmn: (oa,:L/,:ao) PACT
Min RRF for SPCC(#l = 1:1.300 (_0.:50 for BromoformJ Max %PSD for CCC(*) = 30.0"
:LAB FILE ID: RF'F20 = ES0531V03 RRF50 = ES0531V02 ------
: PRF 100= ES0531 V04 RF:F 150= ES0531 \/05 P.F~F-::OO= ES0531 VOE,
---------------------------,------,----------------------------------
' ' COMPOUND :F'F'F:O :RRF50 :PF'FlOO:F'RF150:RRF200: RF'F : FSD
:---------------------------:------:------:------:-===--:-==~==:-------:-----
:Chloromethane ______________ # 0.494:
:eromomethane ______________ _
:Vinyl Ct1loride _____________ •
:c.,1,,r,,etf,~ne ______________ _
:Methylene Ct1loride _________ :
!Ac atone ___________________ _
:Carb,,n Disulfide __________ _
0.840:
(l.515:
1 . 340 !
0.8:.::5:
0.615!
: 1, 1-Di ,: h l ,:,r ,:11~t ht?nP. _________ • 1. 1 EA:
:1, 1-Dichloroethane _________ # 1.95€.:
: 1,:::-Di,::hl,:ir,:,ethene (t,:,t.:il )_: 1.14':1:
:Chloroform _________________ * 2.376:
: t,:-01,:hlor,,~tt,ane _________ 2.<)<)7:
::::-Butanone ________________ _
0.546:
1.:71:
0. ':138:
0.516:
1.2.i-.:::
(l, :.::57:
0.72.9!
1. 185:
2. 031:
1. 222: 3.ooo:
1 • 7·34:
0.l)E.7:
0.507:
1), 9·31 :
0.854:
(l, 514:
0.987:
(l.241!
O.E.40:
1 • (l':11 :
1. '303!
1. 120:
:.:: . 78€, :
1. 74'3: o.os1:
0,4':14!
1.01a:
0.882:
(),510:
f).956:
0.145:
0.659:
1. (174:
0.51€.:
o.·:,:.::1:
0.873:
(l, 51)8:
0. ·;J27:
o. 134:
0.599:
1. 039:
1 • 886 : 1 . BE, 7 :
1 • 124 : 1 • 1)8€, :
2.E,'34:
1.E.74:
0.511:
1 . 034 :
0.877:
0. 513: 1), ':"
l.084<S' · ~ o. 320 e·3, s ·
0. 648: ,
1.111: 5.6·
l. '329:
1. 140:
::. 843:
1. 787:
o. l)E,7: o. 0·3:.:::
: 1, 1, t-Tri,:hl,:,r,:,1c?th-,ne ______ : (1.755!
0.831: o. 3•:1·3:
l).7E,7:
t), 310:
0.677:
!), 457:
0.0:2:
0.74·1: 0.723:
2.758:
1.713:
0. 1)6€, :
o. e.se, :
0.708:
0.273:
I). E,E, "3 : I). 7 1 E, :
:Carbon Tetrac,,loride ______ _ I). 844: 0. 74€,: 0.695:
1). 282!
(I. 765:
0.305:
0.717:
0.305:
0.642:
0,4451
0.691: 11.<?:
:Vinyl Acetate ______________ :
:Bromodichloromett1ane ______ _
: 1,:::-0ichloropropane ________ ·~
:cis-1,3-Dichloropropene ____ :
:Trichloroethene ___________ _
:Oibromochloromethane ______ _
:1, 1,:-Trichloroethane ______ : :Benzene ___________________ _
: trans-1,3-J)ichlor,:,propene __ :
:sromofor•~-· _______________ #
14-Methyl-:Z:-Pentanone _______ : ::-Hexanona. _______________ _
:Tetrachloroethene _________ _
0.359:
0.815:
1),375:
1). 313:
1).497:
0.272
0.729
<).315
0.657
0.470
1).698
0. 4 14 : 1). 323
0.777: 0.7'31
0.319
0.573
0. 193
0.147
0.524
0.569
O.E.54
1).960
:1, 1,~,2-Tetrachloroethane __ # 0.926: !Toluene ____________________ * 0.633:
:Chloroben:ene ______________ # 0.916:
IEt~,ylben:ene _______________ •
:styrene ____________________ :
:Xylene (totdl) _____________ :
(1. 405:
1).868:
1). 5-=E,:
(l, ·435
o. ·334
0.562
0. 2'38:
o. 721: o. e,94: o. e.0:::
l 7. E,
4 ••
0.306: 0.294: 0.31)1
1).648: 1).615: 0.613
0.454: 0.427: 0.417 5. (,:
O.E.94:
0,327:
0.7451
0.332:
0.630:
o. 2'37: o. 715:
o. 311:
o. 63'3: o. 581:
0.612
0.296
o.712
0.309
0.56:
I), 331 : 14. 6;
1).748: 4.8:
0.326: 6.::::
o. 634 ~: --£=-=•
0.206:
t).165:
0.485'
0.618
O.E.14
0.'324
0.418
0.8'37
1).535
0. 1 76: 0. 184
0.1351 o. 135
0. 45'3: 0. 431
o. 17-..;,_: -"=---
0. 479: 7.4:
0.538! 0.535: 0.637:
0.590: 0.583: 0.615:
0.871: 0.865: 0.307:
0.407: 0.394: 0.412:
0.862: 0.840: 0.880!
o.s20: o.so:.::: I). 52·3:
25.'3•
4.8,
4. 4t
:.2
4. 1
4 ..... '
:7~luene-d8 ________________ _ l. 187: 0. '?84 ! 1. 058: 1. 076: 1. 052 ! 1. 1)71 : C,, ·?
7.0
l O. E,
:Bromofluoroben~ene _________ : 0.890: o.733: 0.800: 0.823: 0.793: o.aoa:
:1,2-Dichloroethane-d4 ______ : 2.106: 1.624: 1.702: 1.734: 1.714: 1.776:
--------------------------------------------- ------ -----------------1/87 Re, FORM VI VOA
000302
I
I
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I
I
I u1~
I c/~
I
I
I
I
I
I
I
I
I .... ,. . '\ '.
I
I
I
6A ~eystone DC# 06008 -0<4-17
VOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: KEYSTONE ENV, Contract: 179280-04
Lab Code: ~:EYTX Case No.: 06008 SAS No.: SDG No.: C30WA
Instrument JD:5 ~~l~0~0'---Calibrati,on Date(s): 06/14/90 06/14/90
Matrix:(soil/waterl WATER Level: Clow/med) L=O~W~-Column: (pack/cap) PACK
Min RRF for SPCCl#I = 0,300 10.250 for Bromoforml Ma, XRSD for CCCI*) = 30.0Z
:LAB FILE ID: RRF20 = 6S0614V03 RRF50 = 6S0614V02A -
: F:RF I 00= 6S0614V04 RRF 150= 6S06 I 4V05 RRF200= 6S0614V06
' ' '---------------------------------------------------------------------'-----
COMPOUND :RRF20 :RRF50 :RRF100:RRF150:RRF200: RRF : RSD :
!Chloromethane ______________ # 3.877: 3.168: 2.504: 2.532:
:Bromomethane _______________ : 2.313! 2.273: 1.740: 2.003:
:vinyl Chloride _____________ * 1.731: 1.771: 1.674: 1.·335:
:ct,loroethane _______________ :
:Methylene Chloride _________ :
:Acetone ____________________ :
:carbon Disulfide __________ _
: 1,1-Dichloroethene _________ *
:1, 1-Dichloroethane _________ #
: 1,2-Dichl,:itoethene (t,,tal)_:
:Chloroform _________________ *
:1,2-Dichloroethane _________ :
:2-Butanone _________________ :
:1,1,1-Trichloroethane ______ :
:carbon Tetrachloride _______ :
:vinyl Acetate ______________ :
: Bromo._di chl or omet hane _______ :
:1,2-Dichloropropane ________ *
:cis-1,3-Dichloropropene ____ :
:Trichloroethene ____________ :
:Dibromochloromethane _______ :
:1,1,2-Trichloroethane ______ :
:Benzene ____________________ :
:trans-1,3-Dichloropropene __ :
:Bromoform _________________ l
:4-Methyl-2-Pantanona _______ : :2-Hexanone.;. .. _______________ :
Tetrachloroethena _________ :
1,1,2,2-Tau•chloroethane __ #
Toluene ___ ··---------------* Chlorobenzena ______________ # Ethyl benzene _______________ *
Styrene ____________________ :
Xylene (total) _____________ :
0.797: 0,745: 0.698: 0.781:
1.145: 1.029: 0.950: 0.899'
1 . 02s:
2. 101:
o. 941:
3.236:
1).521:
2.044:
0,914:
2.983:
0.711
2.048
0.910
3.156
2.270:
1.948:
<).920:
3. 178:
1,45•3:
4.351:
4. 137:
0.209:
o. 6'36:
0.635:
1.542: 1.356: 1.429
4,571: 3.925: 4,008
4. 351:
0.199:
0.725:
0.699:
0. 990 : I. 00 1 :
0.780: 0.795:
0.367: 0.364:
0,738: 0.748:
0,407: 0.415:
o.738: 0.111:
0.371: 0,349:
0.836:
0.424:
o.51e:
0.845:
0.428:
0.535:
0.713: 0.629:
0.6531 0,642:
0.449:
0.584:
0.613:
0.835:
0.377:
0.826:
0.504:
0.464:
o.:s1::s:
0,6301
0.878:
0.393:
0.841:
0.519l
3.715
0.134
0.641
0.613
0.840
0,728
0.355
0.702
0,507:
0.699:
0.321:
0.010:
0.40:5
0.486
0.572
0.404
0.431
0.313
0.613
0.826
0.369
0.800
0.484
3.828
o. 182
0.623:
0.586:
0.997:
0.122:
0.379
0.733
0.457
0.694
0.326
0.871
0.418,
0.472:
0,557: o. 532'
0.431
0.367
0.635
0.834
0,373
0.806
0.489
2.379:
2. 161:
1.837:
o.eoo:
0.940:
0.663:
1. 863:
o. 861:
3. 101:
1.411:
4. 197:
4.041:
o. 173:
0.634:
0.612:
0.958:
0.712:
0.351:
0.708:
0.376:
0.676
0.303
0.813
0.405
0.482
0.509
0.:539
0.403
0.480
0.601
0.807
0.359
0.779
0.476
2. 892: 21. 8#
2. 098 : 1 ! . 1 :
1. 790: 5.6•
0. 764: 5.6:
0.993:~,
1. 0~: 68. 7,:
2.001. --7:
0.909:
3. 131
1. 43'3
4,210
4,014
0.179
0.664
0.629
0.957
0.747,
0.363:
0.726:
0.432:
0.716:
0,334:
0.837:
0.416l
0.499'
0.596
0.554
0.436
0.4:52
0.618
0.836
0.374
0,810
0.494
3.2•
3. I#
4.8:
6.2•
6.3:
16.:2:
6.7:
e.. 8:
7. I :
s.o:
3.0•
11. 8: s. 4:
7.9:
2.a:
2.6:
5.3#
13. l :
18. 2: s.2:
24.4#
2.2•
3.1#
3.3•
·3.0:
3.5:
===========================================================================: Toluene-dB _________________ : 1,179: 1,030: 1.032: 1,0191 1.029: 1.058: 6.4:
Bromofluorobenzene _________ : 0.852: 0.739: 0.710: 0.685: 0.704: 0.738: 9.0:
1;2-Dichloroethane-d4 ______ : 4.206: 3.848: 3.441l 3.403: 3.711: 3.7221 e.e:
I I I I I I I ---------------------------·------·------·------·------·------·------·---FORM VI VOA 1/87 Rev.
000406
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7A Key~tone OCtl 06008 -<>4-17
VOLATILE · 1:0NTI NU l NG CALI BRA Tl ON CHECK
Lab Name: KEYSTONE ENV. Contract: 173280-04
Lab C•ode: KEYTX
Instrument ID: 4000
Case N,o. : OE.008 SAS N,o.: SDG N,o. : C30WA
Calibration date: 06/08/30 Ti me : "'O_,,Bee5c,3'---
Lab File ID: ESOE,08V02 !nit, Calib, Date(s): <)6/07/90 06/07/30
Matri,;: (soil/.iater) SOIL Level: (10.,/med) ~L:O~W __ Column: (pack/cap) PACK
Min RRF50 for SPCCCtl) = 0.300 (0.250 f,or Bromaform) Max :t.D f,,r CCC(*! = ~.Ol:
COMPOUND : RRF :RRFSO / 7.0
:Chloromethane ______________ #
:sr~momethane ______________ _
:vinyl Chloride _____________ *
0.556: 0.56~}.;j' 0.764: 1.32 ,-7 .3
o. ·355 ! 0.95.;,, ;"2 *
!Chloroethane ______________ _ 0.529: 0.480: 9.3 :
!Methylene Chloride _________ !
Acetone ___________________ _
Carbon 01sulf1de __________ _
I, 084 1. 124: -3.7 ' ' 0.350 0.187:~:
2.389 2.430: . :
1,1-Dichlaroethene _________ * 1. 095 1. 172: -7.0 4
1,1-Dichloroethane _________ tl 1,387 2.12s: -6.9 ti
1,:-0ichl,:,roethene (total)_: I. I 7 I 1.259: -7.5
Chloroform _________________ • 2.799: 3.003! -7.3 * 1,2-Dichloroethane ________ _
:2-Butanone ________________ _
: 1,1, I-Trichloroethane _____ _
I. 7E,4 1. 789 : :=I:{; o. 103 o. 073(--29. I,
0.798 0. 809 ~
:carbon Tetrachloride ______ _ 0.847 <).814 3.9
:Vinyl Acetate _____________ _ 0.368 0,319 13.3
:Bromodichloromethane ______ _ 0.790 0.790 o.o
:1,2-Dichloropropane ________ * 0.320 0.328 -2.5 ..
:cis-1,3-Dichloropropene ____ ; 0.684 0.697 -1.9
:Trichloroet>,ene ___________ _ 0.462 0.483 -5.8
: Di bromochl i::,romethane ______ _ 0.729 0.709 2.7
:1, 1,2-Trichloroethane ______ : 0.340: 0,323, 5. 0
!Benzene ___________________ _ 0.774: 0,819! -5.8
trans-1,3-Cichloropropene __ : 0.342: 0.339! 0.9
Bromoform __________________ l 0.636: 0.555: 12.7 ti
4-Methyl-2-Pentanone _______ :
2-Hexanone _________________ :
,. Tatrachloroethene __________ :
r ;,-a 1,1,2,2-Tatrachloroethane __ l
0.211: 0.162:~: o. 195: 0.137: 9. 7,,,:
0.503: 0.552: . 7 :
0.669 0.5:541 17.2 • Toluene ____________________ * 0.644 0.695: -7.9 ...
Chlorobanzena ______________ l 0.91:5 0.9971 -9.0 • ,Ethyl benzene _______________ * 0.439 0.488l-11.2 4
:Styrene ____________________ : 0.904 0.962: -6.4
:Xylene (total> _____________ : 0,537 o.seo: -0.0
:================================================:
:Toluene-dB _________________ : 1,037: 1,0191 1.7
lBromofluorobenzene _________ : 0.789: 0.780: 1.1 :
:1,2-Dichloroethane-d4 ______ : 1.685l 1.663: 1.3 :
I I t I I '---------------------------·------·------·------'
FORM VII VOA 1 /87 Re
000432
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l)OC.
7A Keyst,;ne OC# 06008 --<:-1-1
VOLATILE CONTINU!Nt3 CALIBFATION CHECK
Lab Name: KEYSTONE ENV. Contract: ! 79280-04
Lab C,:,de: KEY TX Case No.: 06008 SAS No.: SOG No.: C30WA
Instrument ID:4 ~~O~O~O~--
Lab File ID: E50609V02
Calibration date: 06/09/90 Time: !047 ~~--
Init. Calib. Date(,;'J: 05/31/'?0 05/31 /90
Matri•: (so,1/waterl WATER Level: (!ow/medl ~L=O=W __ Column: (pack/cap) PACK
Min RF:F"50 f,:,r SPCC(#) = 0.300 (0.250 f,:,r Br,:imof,:n•·m) Max 'l.C f,:ir CCC(*) = :ZS.(
------------------------------------------------: :
COMPOUND : RRF :RRF50 : i.D
;~~~~;~:=;~=~=::::::::::::::~=~~;77;=~~;;=:=4~
:sromomethane _______________ 1.034: 1.45 :-4n ·i
:vinyl Chloride _____________ * 0.877: 1.02a:-11.2 *
:Ch!oroethane _______________ 0.513: 0.5371~-~-~
:Methylene Chloride _________ : 1.084' 1,503 -38,6
:Acetone ____________________ 0.320 0.246!~~~~
:carbon Disulfide 0.648 2.4871,-99,9
: I, 1-Di-:h!or,oethe;:;;;=========· !. !II I. !86:'-=e..s "
:1, 1-Dichloroethane _________ # 1.929 2.223:-15.2 #
:1,2-0ichloroethene <totall_: 1,140 1.297:-13.8
:Chloroform _________________ * 2.843 3.117: -9.6 •
/1,2-Dic~,lor,:•ett,ane _________ : 1.787 1.8'33: -5,9:
12-Butanone _________________ 0,092 0.061(~~:~:
:1,1,1-Trict,loroethane ______ : 0.716 0.822:-.8 :
!Carbon Tetrachloride _______ 0.765: 0,916:-19,7
:vinyl Acetate ______________ : 0,305: 0.3471-13.8
:Bromodichloromethane _______ 0.717: 0.8081-12.7
:t,2-Dichloropropane ________ * 0.305: 0.334: -9.5 •
:cis-1,3-Dichloropropene ____ : 0.642: 0,6911 -7.6
:Trichloroethene ____________ 0.445: 0.493:-10.a
:Oibromochloromethane _______ 0.691l 0.721: -4.3
: 1, 1,2-Trichlorc,et.hane ______ : 0.331: 0.328 1 0.9
!Benzene ____________________ 0,748' 0.834 -11.5
ltrans-1,3-Dichloropropene __ : 0,326 0.338 -3.7
:Bromoform __________________ # 0,634 0.539 15.0 #
:4-Methyl-2-Pentanone _______ : 0,227 0.171 24,7
.. :2-Hexanone_________________ 0, 179 O. 130 ~•
:Tetrachloroethene 0.479 0.600 5.3 :
< ------------11, 1, 2, 2-Tet r achl or oet hane __ # 0,637 0,597 • #
:Toluene ____________________ * 0,615 0.686:-11,5 •
:Chlorobenzene ______________ # 0,907 0.991: -9.3 #
:Ethylbenzene _______________ * 0,412 0.4751-15.3 •
:styren~ ____________________ : 0.880 0.946: -7.5
:Xylene <total> _____________ : 0.529 0.501: -9.8
:================================================:
:Toluene-dB : 1.0711 0,995: 7.1
:Bromofluorobenzene _________ : O.BOBl 0.766: ~.2 :
:1,2-Dichloroethane-d4 ______ : 1.776: 1,729: 2,6 :
• • ·---------------------------------·------------
FORM VI I VOA 1/87 R
000438
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7A i<eyst,,ne DC# 06008 --04-J :-
VOLATILE CONT I NU I NO:, CALIBRATION CHECK
lab Name: KEYSTONE ENV.
Lab C,ode: KEY TX Case No.: 06008
Contract: 179280-04
SAS No,: SDG No.: C30WA
Instrument ID: ~4~0~0~0"---
Lab File ID: ES0611V02
Calibration date: 06/11/90 Time: 082!; ~=~--
!nit. Calib, Date(s): 06/07/90 06/07/90
Matrix: (soi I /1.,ater) SOIL Level: (low/med) l~O~W~_
Min RPF50 for SPCCC#) = 0.300 (0,250 f,or Brom,of,ormJ Max Y.D f,or CCC(♦J = 25.0:,
------------------------------------------------:
COMPOUND : R~:F : RRF:SO : Y.D
: Chl ,:,r ,:imethane ______________ # c). 556:
:Bromomethane _______________ 0.764:
!Vinyl Chloride _____________ * 0.955:
: Chi ,,r,oethane_______________ 0. 529:
!Methylene Chloride _________ : 1.084:
:A~etone ____________________ O.3SO:
:carbon Disulfide ___________ 2.389:
:1,1-0ichl,:iroethene _________ * 1.095!
:1, 1-Dichloroethane _________ # 1,987:
:1,2-Dichloroethene (t1.:ital)_: 1.171:
lChloroform _________________ * 2.799:
:1,2-0ichloroethane _________ : 1.764:
::-Butanone _________________ 0.103:
: 1, 1, 1-Tri,:hl,::,r,::iethane ______ : 1). 798:
:Carbon Tetrachl,or1de _______ 0,8471
:Vinyl Acetate ______________ : 0.368:
:Bromod1chloromethane _______ 0.790:
:1,2-Dichl,oropropane ________ + 0.320
:cis-1,3-Dichl,::,ropropene ____ : 0.684
'Trichl,oroethene ____________ 0,462
Dibromochloromethane _______ 0,729
1, 1,2-Trichl,::,roethane ______ : 0.340
Benzene ____________________ 0,774
trans-1,3-Dichloropropene __ : 0,342
Bromoform __________________ # 0.636'
4-Methyl-2-Pentanone _______ : 0,211
2-Hexanona _________________ 0.195
Tetr•chloroethene __________ 0.503
11,1,2,2-Tatrachloroethane __ # 0.669
Toluene ____________________ * 0.644
Chlorobenzene ______________ l 0.915
Ethylbenzene _______________ * 0.439
Styrene ____________________ : 0.904
Xylene (total) _____________ : 0,537
1.123!-17.6 *
1). 5€.7:
1.678 -54.8
0.317: .4
::::. 747:-15.0
1.245:-13, 7 +
2.308!-16.2 #
1.374:-17.3
3.303:-18.0 *
I. 983 :~-,:
0,062: 39.8 :
o. 880: - . 3 :
0.001: -4.o o. 342: 7. 1
0.859: -8.7
o.360:-12.5 +
0.744' -8.8
0.526 -13.8
0.733 -0.5
0.336 1.2
0.871 -12.5
0.354 -3.S
0.548 13.8 #
0.164 ~: 0.116, 40.5 :
o.~e6:-. :
O. 554 17. 2 I
0.732 -13.7 •
1.039 -13,6 I
0.487 -10,9 •
0.975 -7.9
0.597 -11.2
================================================I Toluene-dB _________________ : 1.0371 1.0701 -3.2
Bromofluorobenzene _________ : 0.789: 0.804: -1.9 I
1,2-Dichloroethane-d4 ______ : 1,6851 1.759: -4.4 :
I I I t ---------------------------·------·------·------·
FORM VI I VOA 1 /87 Re,
000446
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7A Key st <>n• DC• 06<)08 -04-17
VOLATILE CONTINUING CALIBRATION CHECY-
Lab Name: 1<:EYSTONE ENV. Contract: 179280-04
Lab C,ode: l<EYTX Case No.: 06008 SAS No.: SOG Na.: C30WA
Instrument !0:4 ~~O~O~O~--
Lab File ID: ES0612V02A
Cal ibrati,on date: 06/12/90 Time: 1310 ==~--
!nit. Calib. Date(s): 06/07/9<) <)6/07 /90
11atri '" <soil /.,ater) SOIL Level: llo.,/med) LOW =~-Column: (pack/cap) PACK
Min RRF50 for SPCC(tl) = 0,300 <0.250 far Bromoform) Max Y.D fQr CCCI*) = ~.07.
------------------------------------------------' .
COMPOUND ; RRF :RRF50 : Y.D
:---------------------------:-----=:------:------:
:Chloromethane ______________ # 0.556:
:Bromomethane _______________ 0,764
:Vinyl Chloride _____________ * 0.955
:Chloroethane _______________ 0.529
:Methylene Chloride _________ : 1,084
:Acetone ____________________ 0.350
:Carbon Disulfide ___________ 2.389
:1,1-Dichloroethene _________ • 1.095,
:1, 1-Dichloroethane _________ tl 1.387:
:t,2-Dichloroethene (totdl)_: t.171l
:Chloroform _________________ • 2.799:
: 1,2-Dichlorc,ethane _________ : 1. 764:
::-Butanone _________________ 0.103:
:1,1,1-Trichloroethane ______ : 0.798:
:carbon Tetrachloride _______ 0.847'
:Vinyl Acetate ______________ : 0,368
:Bromodichloromethane _______ 0.790
:t,2-Dichloropropane ________ * 0.320
:cis-1,3-Di~hloropropene ____ 0.684
:Trichloroethene ____________ 0.462
Oibromoch!oromethane _______ 0.729
1,1,2-TrichlQroethane ______ 0.340
Benzene ____________________ 0.774
trans-1,3-Dichloropropene __ 0.342:
Bromoform __________________ l 0.636:
4-Methyl-2-Pentanone _______ ; 0.2111
,2-Hexanone _________________ 0.19:51
..,;.1Tetrachloroethene 0.503:
-~11, 1,2,2-T•trachlo;;;;;th:;~;;==• 0.669:
··· !Toluene * 0.644:
_._ ': Chl or obenzene ______________ I O. 915 l
:Ethylbenzene _______________ * 0.4391
:Styrene ____________________ : 0.9041
:Xyl~ne (total) _____________ : 0.5371
o. 476: 1".,..;L,tl
!. 30 1 tf-70. 3":
o. 797'!--re'5 • o. 461 : 12. 8
!. 064: 1.8
o. 239: 31. 7
2.196: 8.J
!. 153: -5.8 ¼
2. 113: -6. 3 #
1. 278: -9. 1
3.048: -8.9 *
1.000: -""~:
o. 067 • 6:--o,,/:
o. 807 Cr.-1 :
0.818 3.4
0.319 13.3
o. 797 -o. 9
0.327 -2.2 *
0.702 -2.6
0.505' -9.3
0.747 -2.5
0.340 o.o
0.825 -6.6
0.346 -1.2
0.597 6.1 I
0.172 18.5
0.139 fa':,
0.584 -~
0.601: 10.2 I
0.7151-11.0 *
I. 0401-13. 7 I
o.491 :-11.0 "
0.99:5:-10.1
0.603:-12.3
!===============================================a:
:Toluene-dB _________________ 1.0371 1.0121
:Bromofluorobenzene _________ : 0.7891 0.750:
11,2-Dichloroethane-d4 ______ : 1.6851 1.6251
' ' ' ' ' '
f'ORM VI I VOA 1 /87 Rev
000452
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7A Keystone oc• 06008 -04-17
VOLA Tl LE , (ONT! NU I NG CAL I BRAT I ON CHECK
Lab Name: KEYSTONE ENV.
Lab Code: KEYTX Case No.: 0£008
Contract: 179280-04
SAS No.: SDG No.: C30WA
Instrument ID: 4=0~0~0'-----
Lab File ID: ESOE'.!4V02A
Calibration date: 06/14/90 Ti me: ,.1 _,_1_,_1.:,4c_ __
!nit. Calib. Date(s): 06/07/90 06/07/90
Matrix: (soil /water l SOIL Level: (low/med) L_o_w--Column: (pack/cap) PACK
Min RRF50 for SPCCCeJ = 0.300 <0.250 for Bromoforml Max XO for CCCI*! = ~.0%
------------------------------------------------: : :·
COMPOUND : RRF lRRF50 : XO
:Chloromethane ______________ # 0.556:
:Bromomethane _______________ 0.764:
:Vinyl Chloride _____________ * 0.9551
: Chl ,:iroethane_______________ 1). 529
o. 561 l ~ e
1.5:20~:
1.016: -6. 4 +
0.553: -4.5 : / 11 (o/11/)
0 usr1 .,,-\ /
:Methylene Chloride _________ : 1.084
:Acetone ____________________ 0.350
:carbon Disulfide ___________ 2.389
I. 252: :::J-5· 5 :
o.1sor ~:
3.110(1-30._2 I
I. 1 68 !'--=1,. 7 *
2.0041 -0.9 It
1.235: -5.5
2.973: -6.2 *
1. 762: ~'.?-:h: o. 057 l( 44.? l
o.&94:---n:-o :
0.721 14.9
0.303 17.7
0.685 13.3
0.255 20.3 +
0.555 18.9
0.439 5.0
0.647 11.2
0.284 16.5
0.669 13.6
0.290 15.2
0.617, 3.0 It
0.197:~•'
0.135: 30.8
'I:-
:1,1-0ichloroethene _________ * 1.095
:1,l-Dichloroethane _________ e 1.987
: t, 2-Dii:hl oroethene (t,:ital) _: 1. 171
:Chloroform _________________ * 2.799
: 1, 2-0i •:hl or,:iethane _________ : 1. 764
:2-Butanone _________________ 0.103:
:1,1,1-Trichloroethane ______ : 0.7981
:carbon Tetrachloride 0.847:
'Vinyl Acetate ______________ : 0.368'
Bromodichloromethane 0.790
1,2-0ichloropropane ________ * 0.320
cis-1,3-Dichloropropene ____ : 0.684
Trichloroethene ____________ 0.462
Dibromochloromethane _______ 0.729
1,1,2-Trichloroethane ______ : 0.340 Benzene ____________________ 0.774
trans-1 1 3-Dichloropropene __ : 0.342 Bromoform __________________ e 0.636
4-Methyl-2-Pentanone _______ : 0.211
2-Hexanone _________________ : 0.195
"'.;'·, .JTetrachloroethene __________ 0.503 ~· a, 1, 2, 2-Tetrachloroethane __ e O. 669
_c,,,·rToluen• + 0.644
-·. : Ch 1 or ob•nz ene ______________ # 0. 91 S
lEthylbenzene _______________ * 0.439
:Styrene ____________________ : 0.904
:Xylene <total) _____________ : 0.537
o. 609: - • 1 :
0.641 I 4.2 It
0.7241-12.4 +
0.958: -4.7 I
0.446: -1.6 +
0.936: -3.5
o. 6001-11. 7 :--=-----=-------------==-----------===-===--==--:Toluene-dB _________________ : 1.037: 1.0361
:Bromofluorobenzene _________ : 0.789: 0.732:
:1,2-Dichloroethane-d4 ______ : l.685l 1.6161
0. I
7.2
4. 1
I I I I ·---------------------------·------·------·------
FORM VI I VOA 1/87 Re,
000458
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7A Keystone OCI 06008 -04-17
VOLATILE,CONTINUING CALIBRATION CHECK
Lab Name: KEYSTONE ENV. Contract: 179280-04
Lab C,ode: KEYTX Case No.: 06008 SAS No.: 501, No.: C30WA
Instrument 10: ~4~0~0~0.__ __
Lab File !D: ES0615V02
Matrix: (s,Jil/water) WATER
Calibration date: 06/15/90 Time: 1137 ~=---
!nit. Calib. Oate(s): 05/31/90 05/31/30
Level: (low/med) L.o.w--Column: (pack/cap) RACK
Min RRF50 for SRCC(tl) = 0.300 <0.250 f,or Br,,moform) Max ½O for CCC<•> = 25.0%
COMPOUND : RRF RRF50 : ½0 :===========================:====== ======:======:
:Chloramethane # 0.511
:Bromomethane ______________ _
:vinyl Chloride _____________ *
:cf,loroethane ______________ _
:Methylene Chloride _________ :
1.034
0.877
0.513
I. 084
:Acetone ____________________ 0.320 :carbon Disulfide ___________ 0.648
: 1,1-Dichloroetf,ene _________ * 1.111
:1, 1-0ichlaraethane _________ l 1.929
: 1,:-0i,:hl,:n",:iethene (t,:ital)_: 1.140
:Chloroform _________________ * 2.843
: 1,2-Dichlor,,ethane _________ : 1.787:
:2-Butanone _________________ 0.092:
: 1,1,1-Trichloroethane ______ : 0.716:
:carbon Tetrachloride _______ 0.765: :Vinyl Acetate ______________ : 0.305:
:Bromodichloromethane _______ 0.717:
'1,2-0ichloropropane ________ * 0.305
cis-1,3-0icfiloropropene ____ : 0.642
Trichloroethene ____________ 0.445
Oibromochloromethane _______ 0.691
1,1,2-Trichloroethane ______ : 0.331 Benzene ____________________ 0.748
trans-1,3-0ichloropropene __ : 0.326 Bromoform __________________ # 0.634
4-Methyl-2-Pentanone _______ : 0.227'
2-Hexanone _________________ 0.179
Tetrachloroethene __________ 0.479
1,1,2,2-Tetrachloroethane __ # 0.637
Toluene ____________________ * 0.615
Chlorobenzene ______________ # 0.907
Ethylbenzene _______________ * 0.412
Styrene ____________________ : 0.880
Xylene <total) _____________ : 0.529
0.573:-12.1 #
0.886: 14.3
1).688: 21.6 *
o. 447; 12. 9
1. 171: -8.0
0.337:
2.245:
1 . 202 ,'-...,""
2.107 -9.2#
1. 304 -14. 4
2.714 4.5 *
I. 547 13. 4 o. 101 -9. 8
O. E,44 10. 1
0.582 ~~: 0.412 35. , :
o. 647 • 8 :
0.359 -17.7 *
0.657 -2.3
0.472 -6. 1
0.570 17.5
0.357 -7.9
0.862 -15.2
1).309
0.418
0.240 o. 165
0.509
0.707
0.721
1.000
0.467
0.987
0.592
- • 7
7.8
-6.3
-11.0 I
-17,2 *
-10.2 I
-13.4 *
-12.2
-11.9
----=-=----=--=-------------------==-=----==-m=•:
Toluene-dB _________________ 1.0711 1.0191 4.9
:sromofluorobenzene _________ : o.aoa: 0.6911 14.~ :
:1,2-Dichloroethane-d4 ______ 1 1.7761 1.3921 21.6 I
I I I I ___________________________ • ______ • ______ , ______ 1
FORM. VI I VOA 1/87 Rev
000464
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:--:-·•.·:.:~ .. :-.:
68 l<'.eyst,:,ne DCII 06008 -04-17
SEMIVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: KEYSTONE £NV. Contract : 1 7'3280-04
Lab C,ode: KEYTX Case No.: 06008 SAS No.: SDG No.: C30WA
Instrument ID:4 ~~5~3~0 __ Calibration Date(sl: 06/18/'30 06/ l 8/'?C
Min RRF for SPCC(#) = 0.050 Max 'l.RSD for CCCC•l = s~.O'l.
---------------------------------------------------------------------:LAB FILE ID: RRF20 = ES0618C03 RRF50 = £S0618C02
:RRF80 = £S0618C04 RRF120= ES0618C05 RRF160= ES0618C06
' ---------------------------------------------------------------------· : : : : :
COMPOUND :RRF20 :RRF50 :RRF80
:---------------------------:------:------:------
:P~ienol _____________________ *
:bis(2-ChloroethyllEther ____ :
:2-Chlorophenol _____________ :
:t,3-Dichloroben:ene ________ :
:1,4-Dichloroben:ene ________ *
:Ben:yl Alcohol _____________ :
:t,2-Dichloroben:ene ________ :
:2-Methylphenol _____________ :
:bis(2-Chloroisopropyl)Ether:
:4-Methylphenol _____________ :
:N-Nitroso-Di-n-Propylamine_#
:Hexachloroethane __________ _
:Nitrobenzene ______________ _
: Isophorone _________________ :
:2-Nitrop•ienol ______________ *
:2,4-Dimethylphenol _________ :
:Benzo1c Acid ______________ _
:bis(2-Chloroethoxy)Methane_:
:2,4-Dichlorophenol _________ *
/1,2,4-Trichlorobenzene _____ : :Naphthalene ________________ :
:4-Chloroaniline ____________ :
:Hexachlorobutad1ene ________ *
:4-Chloro-3-Methylphenol ____ *
l2-Methylnaphthalene ________ :
'Hexachlorocyclopentadiene __ #
2,4,6-Trichlorophenol ______ *
2,4,S-Trichlorophenol ______ l
2-Chlorornap~thalena ________ l
2-Nitroanfline __________ _
Dimethyl ·Phthalata _________ l
Acenaphthylene ___________ l
2,6-Dinitrotoluene _________ : 3-Nitroaniline ____________ _
Acenaphthene _______________ *
2,4-Dinitrophenol __________ #
4-Nitrophenol ______________ #
2.440: 1.so2: 1.11s
2.241: 1.65'3: 1.601
1.790: 1.343: 1.272
1.'36'3: 1.578: 1.531
1 . '360: 1 . 558: 1. 4 70:
0. 131 : 0. 08 1 : 0. 360 :
1. 845: 1. 531 : 1. 4'32 !
1 • 7 15: 1 . 534: 1 . 385:
5.580: 4.4121 4.602:
1. 6E. 1 : 1. 272: 1. 408:
1. 5·33:
0.72'3:
0.4'35:
1.037:
0.236:
o. 401:
0.757:
0.338
0.373
1. 253
0.402
o. 170
0.317
1. 120
0.235
0.359
1. 519
1.446
2.200
0.276
1. 1 '34 :
0.593:
0.376'
0.821
o. 186
0.311
o. 130
0.590
0.246
0.308
0.986
0.303
0.143,
0.236:
0.856:
0.2261
0.294'
0.361
1. 231
0.363
1. 183
1. 682
0.249
0.3531
1 • 403 , 1 • 080 I o. 067:
0.055:
1. 273:
0. 61)3 I
0.401
0.907
o. 193
0.335
o. 133
0.640
0.270
0.289
0.976
0.418
o. 127
0.268
0.911
0.204
0.290
0.306'
1. 168
0.388
1. 112
1.676
0.237
0.362
1. 052
0.074
0.051
' ' . ---------------------------'------·------·------
FORM VI SV-1
RRF120:RRF160: RRF : PSD : ---: --: ------: ----:
1.572: 1.585! 1.835: ~9.3*
1.406: 1.314: 1.644: ::::.o:
1. 233: 1 . 133: 1 . 354 : l S. 8:
1. 432: 1 . 3'37 ! 1 . 581 / : 4. 5:
1.4111 1.3861 1.557:~
0.354: 0.420: 0.269:~
1.373: 1.349! 1.518: 13.1:
1. 282 ! 1 . 210: 1. 425: : 4. 2:
4. I 70: 3. '389: 4. S51 : l 3. 6:
1.201: 1.242: t.374: !c.6:
1. 273 : 1 . 368 l 1 . 340: ! ! . 5#
0. 551 0. 51 7 : 0. 599 ! l 2. 4 :
0.479 0.485: 0.447: 1:.2:
0.876 0.836: 0.895: 9.6:
0.217 o. 199: 0.206: 1.8•
0.341 0.328: 0.343: :o.o:
0.145 0.113! 0.130: !0.2:
0.586 0.572: 0.62'3: 12.1:
0.279 0.267 1 0.200: 1:.4•
0.287 0.271 0.306:. !3.0:
0.968 0.8'31 1.015' !3.6:
0.414 0.405 0.388 lc.4:
0.129 0.119 0.138 !4.5*
0.275 0.259 0.271 !0.'3+
0.886' 0.829 0.920 12.6:
0.216 0.208 0.218 5.'3ij
0.315 0.314 0.314 8.7*
0.310 0.284 0.315: 10.3:
1. 111 1. 055 1. 217 14. 9:
0.380 0.357 0.372 3.9:
1. 06:3 1. 009 I. 163 14. 7 :
1.679 1.589 1.765 14.0:
0.244 0.232 0.248 6.91
0.368 0,350 0.358 2.3:
1.014, 0.955 1.101, 15.9•
0.0041 o.0001 0.010: 12.2t
0.0561 0.0561 0.0541 4.4t
---------------------
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l)tJC.
7B Keyst ,one DCM 06008 -:4-1 7
SEM!VOLATILE CONTINUING CALIBRATION CHECK
Lab Name: KEYSTONE ENV. Contract: 173280-04
Lab Cude: KEYTX Case No.: OE,008 SAS No.: SDG No.: C301-/A
Instrument ID:4 ~~5~3~0 __
Lab File ID: ESOcl3C02
Calibration date: OE,/13/30 Time: 1045 ==--
!nit. Calib. Datelsl: 06/11/90 Oc/11/30
Min RRF50 for SPCCl#l = 0.050 Max Y.D for CCCl•l = :-5.<)%
------------------------------------------------
COMPOUND : RRF :RRF50 : Y.D
:P~ienol _____________________ *
:bisC2-ChloroethyllEther ____ :
:2-Chlorophenol _____________ :
:1,3-Dichlorobenzene ________ :
:1,4-0ichloroben:ene ________ *
!Ben:yl Alcohol _____________ :
:t,2-Dichlorobenzene ________ :
:2-Methylphenol _____________ :
:bis(2-Chloroisopropyl>Ether: :4-Methylphenol _____________ :
:N-Nitroso-Di-n-Propylamine_#
:He~achloroethane __________ _
:Nitrobenzene ______________ _
: Isophorone _________________ :
::-Nitrophenol ______________ *
:2,4-Dimethylphenol _________ :
!Benzoi( Acid ______________ _
:bisC:-c•,toroethoxylMethane_:
:2,4-Dichlorophenol _________ *
!1,2,4-Tri(hlorobenzene _____ :
:Naphthalene ________________ : :4-Chloroanillne ___________ _
:Hexachlorobutadiene ________ *
:4-Chloro-3-Methylphenol ____ *
:2-Methylnaphthalene ________ :
:Hexachlorocyclopentadiene __ #
:2,4,6-Trichlorophenol ______ *
l2,4,5-Trichlorophenol _____ _
12-Chloronaphthalene _______ _
12-Nitroaniline ____________ _
:Dimethyl Phthalate ________ _
:Acenaphthylene ____________ _
:2,6-Dinitrotoluene ________ _
:3-Nitroaniline ____________ _
IAcenaphthene _______________ *
:2,4-Dinitrophenol __________ #
14-Nitrophenol ______________ #
l . ·382 : I . 316 : 3. 3 *
1.e,e,1: 1.762: -6.1
I. 379: I. 381: -0. l
1.584: 1.536: 3.0
1.488: 1.595:~~ *
1.046: 0.642 1 38.6 :
1 . 530 : 1 • 503 • :
1.460: 1.311 10.2
4.472: 4.145 7.3
1.438: 1.366 5.0
1.438: 1.231 13.8 #
0.627 0.540 13.9
0.334 0.382: 3.0
0.338 0.845: 9.3
0.204 0.192: 5.9 *
0.359 0.324:e·
0.117 0.155: 32.5
0.631 0.570: • :
0.231 0.276 5.2 *
0.293 0.301 -0.7
1.022 0.996 2.5
0.469, 0.387 17.5
0.131 0.139 -6.1 *
0.333 0.269 19.2 *
0.721 0.880 -22.0
0.231 0.153 31.2 I
0.418 0.343 ~· 0.234 0,348 :
l . 157 l, 174 :
0.412 0.365 11.4
1.236 1.208 2,3
1.838 1.638 10.9
0.258 0.253 1.9
0.402 0.366 9.0
1,106 1.066 3.6 *
0.094 0.076 19.2 I
0.070 0.081 -15.7 I
FORM VII SV-1
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'I ·,;.=.,;.-,,:.~.,:::, . ' . . .
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7C Keyst,:,ne c,:11 06008 -0•-17
SEMI VOLATILE CONT !NU I NG CALI BRAT I ON CHECK
Lab Name: KEYSTONE ENV. Contract: 179280-04
Lab C,:,de: k'EYTX Case No.: 06008 SAS No.: SDG No.: C30WA
Instrument ID: ~4~5~3~0'---
Lab File ID: ES06!3C02
Calibration date: 06/13/90 Time: ~10~4i5~--
!nit. Calib. Date(sl: 06/11/90 06/11/90
Min RRF50 for SPCC(#I = 0.050 Max 1/.D f,,r CCC<*) = 25.01/.
------------------------------------------------
PRF IRRF50 : 1/.D
:-====---==------------------==-==!-=====:======
:2,4-Dinitr,)toluene ________ _
:Diethylphthalate __________ _
:4-Chlorophenyl-phenylether_
:Fluorene __________________ _
!4-Nitroaniline ____________ _
:4,6-Dinitro-:-Methylphenol_:
:N-Nitrosodip>1enylamine (ll_*
:4-Bromophenyl-phenylether __ :
1 . 521 :
0.31)():
1. 141:
0.5171
1. 236:
0. 159:
0.083:
0.663:
0.232:
:He~achlor,,ben:ene __________ 0.214l
:Pentachloropt,enol __________ * 0.115:
:P►,enanthrene _______________ 1. 192:
:Anthracene _________________ 1.063:
IDi-n-Butylphthalate ________ : 1.6001
:r1uorantt1ene * 1.02a:
!Pyrene _____________________ :
:Butylbenzylphthalate _______ :
:3,3'-Dichlorobeniidine _____ :
:BenzoCa)Anthracene ________ _
:Chrysene ___________________ :
:bisC2-Ethylhexyl)Phthalate_:
IDi-n-Octyl Phthalate _______ *
!Benzo(b)Fluoranthene ______ _
!Benzo(k)Fluoranthene ______ _
lBenzo(a)Pyrene _____________ *
!lndenoCl,2,3-cdlPyrene _____ :
:Dibenz(a,h)Anthracene ______ :
:Benzo(g,h,i)Perylene _______ l
1.753:
1. 034:
0.307:
I. 296 !
0.964
1.510
2.983
1.482
1. 072
1.255
1.145
1. 024
1.065
1.401: 7.9
0. 286 l 4. 7
I • 129 : I • I
0.532: -2.9
1.131!~ 0.2~0: '?
0.114:-. :
0. 585: I 1. 8 *
0.239: -3.0
0.231:-10.a
0.110: 4.3 *
1.112 6.7
1.138 -7.1
I. 623
I. 097
1. 568
0.894
0.348
1. 214
0.971
1.397,
2.930!
I. 327:
-1.4
-6.7 *
10.G
13.5
-13.4
6.3
-0.7
7.5
1.8 *
10.5
1.2111-13.0
1.177: 6.2 *
0.910! 20.5
0.872: 14.8
0.863! 19.0
================================================ Nitrobenzene-d5 ____________ 0.370! 0.371: -0.3
2-rluorobiphenyl ___________ : 2.249! 2.521:-12.1
Terphenyl-d14 ______________ : 1.119! 1.142: -2.1
Phenol-d~------------------1.915: 1.948: -1.7 2-Fluorophenol _____________ : 1.578: I.GOil -1.5
2,4,6-Tribromophenol _______ : 0.099! 0.121:-22.2
---------------------------------------------
(1) Cannot be separated from Diphenylamine
FORM VII SV-2
001194
1/87 Re,
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1)6C-
7B Keystone DCtl 0600B --;,4-1
SEM!VOLAT!LE CONTINUING CALIBRATION CHECK
Lab Name: KEYSTONE ENV. Contract: 173280-04
Lab C,~de: KEYTX Case N,:,.: 06008 SAS No.: ____ SDG No,: C30WA
Instrument ID: ~4=5=3~0 __
Lab File JD: ES0619C02
Calibration date: OE,/19/90 Time: 0915 ==--
!nit. Calib, Date(s): 06/18/90 06/ I 8/"30
Min RRF50 fer SPCC<~I • 0.050 Max t.D for CCC(*) •
------------------------------------------------' ' COMPOUND : RRF :RRF50 l i.D
:===========================:======:======:======: :P•ienol _____________________ *
:bis(:-Chloroet•1yl)Ether ____ :
::-c,,lorophenol _____________ :
: 1,3-Dichloroben~ene ________ :
:1,4-Dichloroben:ene ________ *
:Ben:yl Alcohol _____________ :
:1,2-Dichloroben:ene ________ :
::-Methylp~1enol _____________ :
!bis(2-Chloroisopropyl)Ether:
:4-Methylphenol _____________ :
:N-Nitroso-Di-n-Propylamine_#
:Hexachloroethane __________ _
:Nitrobenzene ______________ _
t!sop•iorone _________________ :
:2-Nitrophenol ______________ *
:2,4-Dimethylphenol _________ :
:Benzoic A~1d ______________ _
:bis(2-ChloroethoxyJMethane_:
:2,4-Dichlorophenol _________ *
:1,:,4-Trichlorobenzene _____ :
:Naphthalene ________________ :
:4-Chloroaniline ___________ _
!Hexachlorobutadiene ________ *
4-Chloro-3-Methylphenol ____ *
2-Methylnaphthalene ________ :
Hexachlorocyclopentadiene __ #
2,4,6-Trichlorophenol ______ *
2,4,5-Trichlorophenol _____ _
2-Chloronaphthalene _______ _
2-Nitroaniline ____________ _
Dimethyl Phthalate ________ _
Acenaphthylene ____________ _
2,6-Dinitrotoluene ________ _
3-Nitroaniline ____________ _
Acenaphthene _______________ *
2,4-Dinitrophenol __________ #
4-Nitrophenol ______________ #
!.B35: !.828: 0.4 *
1 • 644: 1. 655 : -0. 7
1 • 354: 1. 357 : -(). 2
!. 58 I : !. 511 : 4. 4
1 • 557: 1. 506 : 3. 3 *
0.269: 0.262: 2.6
1.518: 1.465: 3.5
1.425: 1.306: 8.4
4.551: 4.607: -1.2
1.374: 1.314: 4.4
1. 340:
0.59"3
0.447
0.895
0.206
0.343 o. 130
0.629
0.280
0.306:
1.015'
0.388
o. 138
0,271
0.'320
0.218
0.314
0.315
1.217
0.372,
I. 163
1.765
0.248
0.358
I. 101
0.078
0.054
1 • 2'30 : 3. 7 #
0.571: 4.7
0.491: -·3.8
0.875: 2.2
0.203:
0.328: o. 128:
0. 6 I 4:
0.280:
o. 30'3:
0.'367:
0.365:
0.140:
0.267
0.888 o. 171
0.324
0.308
I. 166
0.358
1. 112'
1. 703
0.229
0.333
1.080
0.054
0.056
1.5 *
4.4
1.5
2.4
o.o *
-1.0
4.7
5,9
-1,4 *
1.5 *
3.5
21. 6 •
-3.2 *
2.2
4.2
3.8
4.4
3.5
7.7
7.0
<$.r:
:s. (
FORM VII SV-1 odi~cfif
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I .. ,:,... -.~..-:)
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7C l<eyst,;ne DCtl OE.008 -04-17
SEMIVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: KEYSTONE ENV, Contract: 179280-04
Lab C,ode: KEY TX Case No,: 06008 SAS No.: SDG No. : C30WA
Instrument ID: ~4~5~3~0~--
L.ab File ID: ES0619C02
Calibration date: 06/19/90 Time: 0515 ~=~--
!nit. Calib. Date(s): 06/18/90
Min RRF50 for SPCC(ij) = 0.050
COMPOUND RRF
:Diben:,ofuran 1.461
:2,4-Dinitrotoluene ________ _
!Diethylphth.alate __________ _
:4-Chlorophenyl-phenylether_,
:Fluorene __________________ _
!4-Nitroaniline ____________ _
!4,6-Dinitro-2-Methylphenol_!
!N-Nitrosodiphenylamine Ill *
4-Bromophenyl-phenylether __ :
He~achloroben:ene _________ _
Pentachlorophenol __________ *
Phenanthrene ______________ _
0.262
1 • 040
0.521
1. 133
o. 147!
0.115!
0.686:
0.261:
0.240:
0. 118 !
1. 188 !
Anthracene _________________ 1.122
Di-n-Butylphthalate ________ : l,E.61
,Fluoranthene * 1,027
Pyrene _____________________ :
Butylbenzylphthalate _______ :
3,3'-0ichlorobenzidine _____ :
Benzo(a)Anthracene ________ _
Chrysene ___________________ l
bis<2-Ethylhexyl)Phthalate_:
Di-n-□ctyl Phthalate _______ *
,Benzo(b)F!uoranthene ______ _
!8enzo(k)F!uoranthene ______ _
!Benzo(a)Pyrene _____________ *
:Indeno(l,2,3-cd)Pyrene _____ :
:Oibenz<•,h>Anthracene ______ :
,JBenzo(g,h,i)Perylene _______ :
I. 687
1.011
0.24'3
1. 256
1.042
1,534
3.357
1.451
I, 320
1. 272
0.'365
0.'328
0.'310
RRF50 ! 1.D
1.382: 5.4 o. 253: 3. 4
o. 980: 5. 8
o. 530 ! -1. 7
1.0'34~'"'
0.102 30.6
o.0·39: -.Ja :
O.E.'36! -1.5 *
0.270'
0.262
o. 121
1. 134
1. 105
I. 578
0.985
I, 594
0.'311'
0.245
1. 034
I. 034
I, 385
3.063
1.271
1.271
1 • 1 '34
0.858
0.865
0.022:
-3.4
-9.2
-2.5 *
4.5
1.5
5.0
4. 1 *
5.5
'3. '3
1.6
17.7
0.8
'3. 7
8.8 *
12.4
3.7
6. 1 *
I 1. 1
6.8
'3. 7
:m=============================================== ~lNitrobenzene-d5 ____________ 0.364!
.:2-rluorobiphenyl ___________ : 2,417:
:Terphenyl-d14 ______________ : 1.105!
lPhenol-d5 1,767:
:2-F!uorophenol _____________ : 1.577!
:2,4,6-Tribromophenol _______ : 0.084:
0.385
2.577
1.164
1.888
1.653
0.104
(1) Cannot be separated from Diphenylamine
FORM VI I SV-2
-5.8
-6.6
-5.3
-6.8
-4.8
-23.8
06/18/90
001205
1/87 Rev
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/)uC.
78 ~:eyst one DC# 06008 -v'-1 7
SEMI VOLATILE CONT I NU I NG CALIBRATION CHECK
Lab Name: KEYSTONE ENV. C-ontract: 179280-04
Lab C-ode: KEYTX Cose N,:i. : OE.008 SAS No.: SDG N,,. : C30WA
Instrument ID: ~4~5~3~0 __
Lab File ID: ES0620C02A
Calibration date: 06/20/90 Time: .1~2~1~7 __
!nit. Calib. Date(s): 06/18/"30 06/18/30
Min RRF50 for SPCCC#J = 0.050 Ma:< 1/.0 for CCC<•J = :::-S.O'l.
COMPOUND : RRF !RRF50 : 1/.D
:P►,enol _____________________ *
:bis<2-ChloroethyllEther ____ :
:2-Chlorop ►1enol _____________ :
:1,3-Dichloroben:ene ________ :
:t,4-0ichlorobenzene ________ *
:Benzyl Alcohol _____________ :
:1,2-Dichlorobenzene ________ !
:2-Methylphenol _____________ :
:bis(2-Chloroisopr,Jpyl)Ether:
:4-Methylphenol _____________ :
:N-Nitroso-Di-n-Propylamine_#
:Hexachloroethane __________ _
:N1troben:ene ______________ _
:Isophorone _________________ :
:2-Nitrophenol ______________ *
:2,4-Dimethylphenol _________ :
:sen:01c Acid ______________ _
:bis(2-Chloroethoxy)Methane_:
:2,4-Dic•ilorophenol _________ *
:1,2,4-Trichloroben~ene _____ :
!Nap•ithalene ________________ :
'4-Chloroaniline ___________ _
Hexachlorobutadiene ________ *
4-Chloro-3-Methylphenol ____ *
2-Methylnaphthalene ________ :
Hexachlorocyclopentadiene __ #
2,4,6-Trichlorophenol ______ *
2,4,5-Trichlorophenol _____ _
2-Chloronaphthalene _______ _
2-Nitroaniline ____________ _
Dimethyl Phthalate ________ _
Acenaphthylene ____________ _
2,6-Dinitrotoluene ________ _
3-Nitroaniline ____________ _
Acenaphthene _______________ *
2,4-0initrophenol __________ #
4-Nitrophenol ______________ #
1 . 835: 1. 868: -1 . 8 *
1.644: !.718 -4.5
1 . 354: 1. 388
1 . 581 : 1. 593 -0.8
1. 557:
0.269:
1.510:
1.425/
!.613 ~~:. 0. !55
1. 544
!. 656 -16. 2
4.551! 4.443, 2.4
1. 374: 1. 360: 1. 0
1 , 340 ! 1. ::'39: 3. 1 #
0.539: 0.600: -0.2
0.447 0.362: 1·3.0
0.895
0.206
0.343
0. 130
0.629
0.280
0.306
1.015 o. 388 o. 138
0.271
0.920
0.218
0.314
0.315
1.217
0.372
1. 163:
1.765:
0.248
0.358
1. 101
0.078
0.054
0.855 o. 19'3
0.327
o. 142
0.589
0.287
0.310
0.966
0.351
o. 143 /
0.285:
0.923:
0.200:
0.309:
0.336
1. 141
0.372
1. 150
1. 748
0.256
0.369
I. 071
0.079
0.060
4.5
3.4 *
4.7
-9.2
6. 4
-2.5 *
-1.3
4.8
9.5
-3.6 *
-5.2 *
-0.3
8.3 #
1.6 *
-6.7
6.2 o.o
1.1
1. 0
-3.2
-3.1
2.7 *
-1.3 #
-11. 1 •
FORM VI I SV-1 1/87 Rev
001215
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f)oC,
7C Keystone DC# 06008 -0-1-17
SEMIVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: KEYSTONE ENV. Contract: 179280-04
Lab Code: KEY TX Case N,o.: 06008 SAS N,o,: ____ SD'3 No.: C30WA
Instrument ID: ~4~5~3~0'----
Lab File ID: ES0620C02A
Calibration date: 0£/20/90 Time: 1217 ==---
!nit. Calib. Date<s.l: 0£/18/90 06/18/'30
Min RRF50 f,or SPCCI#) = 0.050 Max 'l.D for CCCI*) = 25.0%
---------------------------,------,-------------' ' COMPOUND : RRF
:Dibenzofuran ______________ _
::.4-D1n1trotoluene ________ _
:Diethylphthalate ___________ :
:4-ChloJrophenyl-phenylether_:
:rluorene __________________ _
:4-Nitroaniline ____________ _
:4,6-Dinitro-2-Met•iylphenol_l
:N-Nitrosodiphenylamine (l)_*
:4-Brom,ophenyl-phenylether __ :
!He~achlorobenzene _________ _
:Pentachlorophenol __________ *
:Phenanthrene :·
I. 461
0.262
I. 040
0.521
I. 133
0. 147 o. 115
0.£86:
0. 261 :
0.240:
0. 118:
I. 188:
:Ant•1racene _________________ 1.122!
:Di-n-Butylphthalate ________ : 1.661:
:~luorant•1ene _______________ * 1.027 1
!Pyrene _____________________ : 1.687
:Butylbenzylphthalate _______ : 1.011
:3,3'-Dichlorobenzidine _____ :
:Benzo(a)Ant•iracene ________ _
lChrysene ___________________ :
:bisl2-Ethylhexyl)Phthalate_:
:Di-n-Octyl Phthalate _______ *
:senzo(b)Fluoranthene ______ _
:Benzo(k)Fluoranthene ______ _
:Benzo(a)Pyrene _____________ *
:Indeno<l,2,3-cd)Pyrene _____ :
:Dibenz(a,h)Anthracene ______ :
:Benzo(g,h,i)Perylene _______ :
;_ : Nit r obenzene-d5 ___________ _
12-Fluorobiphenyl __________ _
:Terphenyl-d14 _____________ _
:Phenol-d5 _________________ _
:2-Fluorophenol ____________ _
:2,4,6-Tribromophenol ______ _
0.249
1. 256
1.042
I. 534
3.357
1.451
1.320
1. 272
0.965
0.928
0.910
0.364
2.417
I. 105
1. 767
1. 577
0.084
RRF50 : %0
----=='======:
1. 405 3.8
0.282 -7.6
1.067 -::.6
0.540 -3.6
1. 135 -0.2
o. 157 -£.8
0. 113 1.7
0.704: -2.6 * 0.258: 1.1
0.243! -1. 2
o. 135: -14, 4 ~
I. 141: 4.0
1. 129: -C). 6
1.610: 3.1
1.04'3: -2.1 I
1.607: 4,7
0.937~' 0.342 -37.4
I. 1 77: • o. 962: 7. 7
I. 40£: 8. 3
3. 232: 3. 7 *
1.418: 2.3
I. 137: 13.9
1.171: 7.9 *
0.864: 10.5
0.852: 8.2
0. 809: 11. 1
0.378: -3.8
2.439: -0.9
1.196: -8.2
2.024:-14.5
1.552: 1.6
0.097:-15.5
Cl) Cannot be separated from Diphenylamine
FORM VI I SV-2
001216
I /87 Rev
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I _;..__ ~--=·~ .1
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7B Keystone DCM OE,008 -o•-17
SEMIVOLATIL~ CONTINUING CALIBRATION CHECK
Lab Name: KEYSTONE ENV. Contract: 173280-04
Lab C,ode: KEY TX Case No.: OE,008 SAS No.: SDG N,o.: C30WA
Instrument ID:4 ~:5:3~0 __
Lab File ID: ESOE,2E,C02
Calibration date: 06/26/90 Time: ~la2~1~7 __
!nit. Calib. Date(sl: OE,/18/90
Min RRF50 for SPCCC#l • 0.050
------------------------------------------------
COMPOUND : RRF
:Phenol _____________________ *
:bisl2-ChloroethylJEther ____ :
:2-Chlorophenol _____________ :
:1,3-Di(hlorobenzene ________ :
:t,4-Dichloroben=ene ________ *
:senzyl Alcohol _____________ :
:t,2-Dichlorobenzene ________ :
:2-Met•,ylp~1enol _____________ :
:bis(2-ChloroisopropyllEther:
:4-Methylp11enol _____________ :
:N-Nitroso-Di-n-Propylamine_#
:He~achloroethane __________ _
:Nitrobenzene ______________ _
:rsophorone _________________ :
::-Nitrophenol ______________ *
l2,4-Dimethylphenol _________ :
:Benzoic Acid ______________ _
:bisl2-Chloroethoxy)Methane_:
:2,4-Dichlorophenol _________ *
:1,2,4-Trichlorobenzene _____ :
:Naphthalene ________________ :
:4-Chloroaniline ___________ _
:Hexachlorobutadiene ________ *
:4-Chloro-3-Methylphenol ____ *
:2-Methylnaphthalene ________ :
:Hexachlorocyclopentadiene __ #
:2,4,6-Trichlorophenol ______ *
:2,4,~-Trichlorophenol _____ _
,.;,,,I 2-Ch_l or onapht hal ene _______ _
·12-Nitroanlllne
,_.:s. -------------._: ,I DI methyl Phthal ate ________ _
lAcenaphthylene ____________ _
12,6-Dinitrotoluene ________ _
:3-Nitroanillne ____________ _
:Acenaphthene _______________ *
12,4-Dinitrophenol __________ #
:4-Nitrophenol _____________ #
1. 835
I. E,44
1. 354
1. 581
I. 557
0. 26'3
1.518:
1. 425:
4. 551:
1.374:
1.340:
0.59'3:
0.447:
o. 8'35:
0.206:
0.343:
o. 130:
0.62'3:
0.280:
0.306:
1.015:
0.388'
o. 138
0.271
0.920
0.218
0.314
0.315
1. 217
0.372
1. 163
1. 765
0.248
0.358
1. 101:
0.078:
0.0541
RRF50 : XO
1.923 -4. 8 *
1.948 -18. 5
1.447 -6.9
1.612 -2.0
1.625 $.i)* 0,813 '9'3.'9 :
1. 544 - . 7 :
1. 335, 6.3
4. 7E,6 -4.7
I. 371 0.2
1. 137 10.7 #
0.654 -'3. 2
0.558 -24.8
0. '370 -8.4
0. 186 9.7 * 0.337 1.7
0. I 17 10.0
0.631 -0.3
0.287 -2.5 * 0.301 1.6
0.998 1.7
0.380 2. 1
0.148 -7.2 * 0.282, -4.1 * 0.949: -3.2
0.134: 11.0 • 0.324: -3.2 * 0.293: 7.0
1. 151: 5.4
0.390: -4.8
1.076: 7.5
1.714: 2.9
0.2221 10.5
0.3361 6. 1
1.071 I 2.7
0.0611 2
0.068' 25.9 ---------------------------------______ ,,._.___.,,.
FORM VII SV-1
OE,/18/30
1/87 Rev
001226
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7C Keystone DC• <)6008 ""'-'-4-17
SEMIVOLAT!LE CONTINUING CALIBRATION CHECK
Lab Name: KEYSTONE ENV. Contract: 179280-04
Lab Cc,de: KEYTX Case No.: 06008 SAS No.: SDG No. : C30WA
Instrument ID: ~4=5=3~0~--
Lab File ID: ES0705C02
Calibration date: 07/05/90 Time:O ~~9~4~6'---
!nit. Calib. Date(s): 06/18/90 06/18/90
Min RRF50 for SPCC(#l = 0.050 Max t.D for CCC<•l = :-5.0%
COMPOUND RRF RRF50 t.D
:D1bencofuran _______________ 1.461 1.269 13.1
:2,4-Dinitrotoluene _________ 0.262 0.278 -6.1
:Diethylphthalate ___________ 1.040 1.022 1.7
:4-Chlorophenyl-phenylether_, 0.521 0.469 10.0
: Fl u,orene___________________ 1. 133 1. 078: ~
:4-Nitroaniline _____________ : 0.147 0.094~
:4,6-Dinitro-2-Methylphenc,l_: 0.115 0.106: 7.8
:N-Nitrosodiphenylamine (1) * 0.686 0.677: 1.3 *
:4-Bromophenyl-phenylether __ : 0.261 0.213: 18.4
:Hexachloroben:ene __________ 0.240 0.226: 5.8
:Pentachlorophenol __________ * 0.118 0.118 0.0 *
:Phenanthrene _______________ 1.188 1.133 4.6
:Anthracene _________________ 1.122' 1.015 9.5
:Di-n-Butylpt,thalate ________ : 1.661 1.823 -9.8
:Fluoranthene _______________ • 1.027 1.175 -14.4 *
:Pyrene _____________________ : 1.687 1.786 -5.9
Butyl benzyl phthal ate _______ : !. 011 0. 993 I. 8
3,3'-Dichlorobenzidine _____ : 0.249 0.210 15.7
Benzo(a)Anthracene _________ 1.256 1.271 -1.2
Chrysene ___________________ : 1.042 1.060 -1.7
bis<2-EthylhexyllPhthalate_: 1.534 1.638 -6.8
Di-n-Octyl Phthalate _______ * 3.357 3.300 1.7 *
Benzo(b)Fluoranthene _______ 1.451 1.324 8.8
Benzo(k)Fluoranthene _______ 1.320 1.101 16.6
Benzo(aJPyrene _____________ * 1.272 1.233 3.1 *
Indeno(l,2,3-cd)Pyrene _____ : 0.965 0.828 1
Dibenz<a,h)Anthracene ______ : 0.928, 0.680, ,<;:=.-,
Benzo<g,h,iJPerylene _______ : 0.910: 0.648:
'======cz==================================-~---•-~=~=
Nitrobenzene-d5 ____________ 0.364: 0.377: -3.6
2-Fluorobiphenyl ___________ : 2.4171 2.446: -1. 2
Terphenyl-d14 ______________ : 1.105: 1.173: -6.2
Phenol-d5 __________________ : 1.767: 1.863: -5.4
2-Fluorophenol _____________ : 1.~77: 1.670: -5.9
2,41 6-Tribromophenol _______ : 0.084: 0.084: o.o ___________________________ : ____________ I _____ _
(1) Cannot be separated from Diphenylamine
FORM VII SV-2
001238
1 /87 Re,
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3A Keystone DCM 06008 -04-lC
w,;TEF: '/OL\TIL'.;; M,HF:::: Sc'lf.:E/MATF:!X SFWE DUF'LIC,HE F'ECOVERY
L~b Name: KEY~TONE ENV.
--: SP HE : SAMF'LE : MS --MS------o,:--
: ADDED :CONCENTF:ATinN:(ONCENTRATION: X :L:MIT~
CCMFOUND fug/U (ug/U rL19/U F·EC 1: ~EC.
1~ 1-Dict,lor,~ethene _____ :
Tri,:t1l,)roett1ene _______ _
Ben~ene _______________ _
~(). ()
51). ()
50. 0
5(1. (J
sn.o
t)
()
0
(l
(l
5·3. '3
2-C,. 0
60. 1
1 20 : 61-14 ':
11:.:: :71-1:::-:
: Sf':KE : MSD MSD -
: ADDED : ,:.ONCENTRAT I ON: ,. 'l. QC LIMIT~.
,:□MPIJUND <'ug/U iug/l) RE•: 11: F:PD #: RPO : •EC. :------------------------:---------:-------------!------:------:------:------
1 1 ·D 1 ,: h 1 ,:or ,:,et hen e 51). 0 55.8 -----1 1 ·' ~ 7 14 :t.t-14~
Tr 1,:h l ,:ir ,:,et hene --------50.0 54.5 10'3 3 14 : 7: -1 :.:.\
Ben::ene ----------------:so. (l 58.8 I 18 2 I I : :-'6-1.::~
T,:il uene ----------------50.0 61. 6 1~~ .;.-., 3 13 : 7e,-1 ·.::":
Chl ,:,r,:,ben..:ene ----------50.(J 58.8 118 3 1: : :-s-1 :.:
tt C,:,lumn to_ be used to flag re,:,:Nery and RPO values with d.n asterisk
• Values outside of QC limits
F:PD: _Q ,,ut of _Ji
Spike Recovery: __ !
(Ot1MENT3:
outside limit5
..:iut of _!Q outside limits
FORM III VOA-1 -.1/8:'Re, 00000!)
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/)(JC.
3Q
SOIL SEMIVOLATILE MATPIX SP!KE!MATP!X SPIKE DUPL!CATE ~ECOVERY
' SPi~.~ l SAMPLE : MS MS--
; ADDED :c□NCENTPATIONICONCENTPATION:
,:□MF·OUND
F·J,enol ________________ _
:2-Ch l ,:,r,:,pher,,:,1 _________ I
t,4-Di,:11lor,~•b211:en~ ____ :
N-Ni t.-·,:,s,:,-di-n-proo., 1 °I;
L , -::_, ·c.J.-Tr-~ ,: :1 : ,:,r" ,:,b ,~n: :::,,n Q _ !
~-Cf1lc,rc,-:-m~t!1yl~i1en0l:
,;,:~n~pf,thcne ___________ :
J-N1tropl1enc,l __________ :
·::. ,--1, ·-0 i r. i t , :, t; ,:, ! :.1,:--n f: _____ _
f·en t ~ch l ,:,r ,:,p t1 en,:, l ______ ! Py,~ne _________________ _
SO·?O
50'?0
"2550
.::sso
5(1':/(J
:255(l
50'.:!0
-~551:•
5c)·3'o
2550
( Ltg /Kg)
0
()
('
1)
0
t)
(J
c) ,.,
•.)
0
4780
4810
:.:: t ·?()
.::1so
:·34c)
5! 1 t)
:."?70
5850
3 1 C:10
SE.1)0
264(1
':14 -+: .:.c-'?
'.:14 : .::-=:-1 (1
86 : .:.·,= 1 (,
8-1 :~, 1.:
~~~~ ~:~: ;'iri-7 : : : -1 2
115 *:::-11
122 •::::s-2
110 •:1~-1,)
104 ::5-14
------------·------------------------·------------------------------------·
-----------------------------------------------------------------------------
·------------·------------' ,--------------------·-------, Pt,encl ________________ _
::-(h I ,:,r-,:,phl?n,:,l _________ :
1,4-0i,:t,lorobenzene ____ :
N-Ni tr,:,so-di-n-pr,:,p. ( l):
1,2,4-Trichloroben:ene_:
4-,:~1l0r0-3-methylphenol:
Acenaphthene ___________ :
4-Nitrophenol __________ ;
2,4-0initrotoluene _____ :
Pentachlor,ophenol :
Pyrene_· ~--------------:
SFH:E
:.;ODED
(u9,·f-\1 "i
:30'3(~
.S(J'j()
·::550
2550
2550
5030
2550
5090
2551)
50':10
·.::sso
(1) N-Nitroso-di-n-propylamine
,'15D
: ,:ori,:EMT?AT ION:
(u9/K9)
4300
431(1
18-10
18"30
2060
5230
2710
5720
2780
5700
2480
f1SD
1/.
f::EC
3-1
85
72
7-1
#I
:: o,: LIie; TS
PF'D ., F:F'[I : :: ::c. . '
1 1 -~ C,.., : :·5-'j1
10 50 : -.:::-1 !)'.
18 27 : ~s 1 O·
13 '.:8 : 4 : l ,:,
13 .23 '~" '.;,.;J l (l-:-
1-1 33 : 21:. 1 ,:,
'3 l '3 ;3~-1:-
-1-1 50 : l ~ - 1 !·
I 1 -17 ::a-8·:
-:: 47 : !7-l(r:
7 3E, :35-14:
» C0lumn t,) bo 1Js~d ti~ flag ,-e~,)·~cry ~nd RPO values wit>, dn ~storisk
• V~lues out!ide 0f QC :imits
F:F'O: ___Q out •:ii _1 L
-~pike F.·e,:,:i·.,1ery: __.1
,:·OMMEN TS:
•::iu t •.5 i d •:i l l ml t 3
,::iut ,:if :::: ,:,1_,tside limits
FORM III SV-2
000601
1/87 Re
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WA TEP SEMI'IOLATic.:': M.;TF:J'( SF If E,'f1ATF:D Sr'IIE DUPLICATE F·E(OVEF··
---------SF·!•(E SAMPLE --~-----~~--------~§------3~-
: ADDED ICONC~NTF'AT!□N:(ONCENTPATION: •• :L:~IT
,:OMPDUND
F·t,~nol ________________ _
2-Cf,loroplien,)l _________ :
l,4-Di~f,l,:,r,)b8n:~n~ ____ :
N-Nitr,:,s,:,-di-n-pr,:,p. < 1};
1.~.4-Tr1cl1lc,r,:,ben:~n~_:
•1-Chloro-3-methylp11enol:
1 ')')
1 (;1:1
50. 1:1
50. (1
: 1)tJ
51). ,:i
i l:iO
5•.:•. 1)
l c":1
50.0
I)
,-,
,_,
(I
1.ug/l)
1 2. 6
17.3
:E,.7
48.8
41. 0
-D.8
> 2 --' ~· . -
I_.:, : :::: :. •:
70 ,-. 11
84 : c: •O·
·;.s :..:.::-1~
27 : : :-2·
55 ; :.:. :-'?·
41 ; ;'-1 !),
lOC, ::c-12·
-------... ----------·-----------------------------
---------------------------------------------------------------------------SP I 1:'E
: ,,ODED
cor1F C:IJND
F·t,enol ________________ _
2-1:t,l,)ropt1enol _________ :
1,4-Dichloroben:ene ____ :
:J-Ni tr,:,~•=•-di -n-pr,:,p. ( 1):
t,:,4-Tri~J,l,)r,.:iben:ene_:
4-Ct,Ior,.:i-3-mett1ylpf1enol:
Acenaphthene ___________ :
4-Nitrop•ienol __________ :
2,4-Dinitrotoluene _____ :
Pentachl6rophenol ______ :
F'yr ene_.::.5-_____________ :
'
(L19/L)
11)()
1 ()(I
50.0
5(). c)
51). (l
1 C)(J
50.0
I 00
50.(l
100
50.0
MSD
: ,: IJrJ1:.ErHF:AT I ON:
•.:ug/L)
85.0
GO. ·':J
36.3
38.€,
-l 1 • 5
'31. ·:1
50. I
E.4. -I
3'3. 8
·j l. 2
51). 1
MSD ., ,.
PEC #: ~:F'D #:
85
81
73
77 ' -10 ' 83
·~ ' ' ·3-.:: : -'::ff) ·:f-
100 ' ' ' E.4 : -81 •
80 ;© "3 !
101) : -:
o,~ Lif".: :-s
,·FD : = c:,: •
-12 : 1:-St
40 ' --1.:::
-:a : ~E ';(
38 : -l : ! 1 I
28 : :·= ·~t
4-~ '_.;. ·:1-
31 1-1£-!lE
50 : 1 (·-S<
38 '~. ·:JE ' ---50 : ·:--10:·
31 : :.>~-1 :2·
---------------------------------------------------------------------
(!) N-Nitroso-di-n-propylamine
~ r~,:,lumn t,:i be u:1t?d t,:, fl.:ig re,.:,:,vcr·i ,.1nd f.:F'D v-=tl1Je'3 \,,lith an .JSterisl-:
~ l/dlue·.5 ,)Lttside ,:,f OC limits
F'F'D: 5 ,:out ,,:if __!_l ,:,utside l im\ t;:;
Spike Peco~ery: __ l out of __ ,,utside li1nits
COMMENTS: l KPD tc.r Phenol and 2-Chlorophenol are -99 on floppy.Formaster doe, not
calculate values beyond -99Chfa,.tf).
f'OF:M III SV-1 ! /87 11ev
00060(
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D
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BB 3E
WATER PESTICIDE MATRIX SPIKE/MATRIX Sf·IKE DUPLICATE RECOVERY
Lab Name: KEYSTONE ENV.
Lab Code: 1-EYTX Case No. : c)':,(ll)8 SAS No.: SDG No. : C30WA
Matrix Spike -EFA Sample No.: c-goA
COMPOUND
SPIKE
ADDED
<ug1u
SAMPLE MS
:CONCENTRATION:CONCENTRATION:
Cug/L) Cug/L)
SF" I kE MSD : MSD
MS DC
¼ :LIMITS:
REC II: REC. :
ADDED :CONCENTRATION: ¼ ¼ QC LIMITS
: COMF·OU!s[I : (ug/L) : (ug/l) : REC II: RF'[, 11: RF·D : REC. ,
:' = gamma-BHC;;:; <Li ndane) __ :: ==== 0 .200; :;:;======= 0 ==== ~= 0 == '.-== 15 ;;=; 5t,-123;
: Heptdchlor _______ : 0.200: 1).160 ~ 7 : 20 :40-131:
Aldi-in__________ 0 .200: 0. lo'! 82 9 22 :<10-12,,:
Dieldrin_________ 0.500: 0.'137 87 9 18 :52-126:
Endrin_________ 0.500: 0.37'1 75 10 21 :s,;-121:
'1,4'-DDT________ 0.500: 0.'199 100 E, 27 :38-127:
II Column to be used to fl•g recovery and RPO values with •n asterisk
• Values outside of QC limits
Rf·D: 0 out of b outside limits
Spike Recovery: 2 out of 12 outside limits
COMMENTS:
001386
FORM III PEST-I 8/87 Rev.