NCD003200383_19870122_Koppers Co. Inc._SERB PA SI_Site Investigation December 1986-OCR

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North Carolina Department of Human Resources
Division of Health Services
P.O. Box 2091 • Raleigh, North Carolina 27602-2091
James G. Martin, Governor
Phillip J. Kirk, Jr., Secretary Ronald H. Levine, M.D., M.P.H.
Ms. Denise Smith·.
EPA NC CERCLA Project Officer
EPA Region IV Waste Division
345 Courtland Street, N.E.
Atlanta, GA 30365
Dear Ms. Smith:
SUBJECT: Summary Trip Report
22 January 1987
Koppers Co., Inc. NC D003200383
Hwy. 54 West
Morrisville, NC 27560
Site Investigation, December 17, 1986.
State Health Director
Tne Koppers Co., Inc. site is located on a 53 acre tract on Hwy. 54
West in Morrisville, NC. A company called Unit Structures first produced
glued-laminated wood products on this site around 1955 until 1962. Koppers
purchased the site in 1962 and continued the glue-laminating process. From
1968 to 1975, Koppers used the southeast portion of the site for wood
_treatment with pentachlorophenol (PCP). Wood treatment was discontinued on
site around 1976, however, laminated wood production continued. The plant was
sold in September 1986. Koppers retained 10 acres of the original site
including the areas where PCP contamination was known or likely to have
occurred. The remainder of the site has been sold back to Unit Structures.
Koppers notified as a generator, transporter at this site. However, no Part A
application for interim status was filed and no closure permits have been
issued.
Wastewater lagoons from the PCP treatment process were closed by
Koppers in 1976. The liquid from the lagoons was sprayed over a portion of a
field in the northeast corner of ·the property and the sludges were mixed with
soil surrounding the lagoons. Soil samples collected by Koppers in the spring
and fall of 1980 led to the removal of PCP contaminated soil from the site.
Subsequent studies have been conducted by Koppers and US EPA Region IV. To
date, PCP has been measured in soil, groundwater, and pond sediment on site.
Ms. Denise Smith
22 January 1987
Page 2
The northern portion of the site drains to a ditch which crosses under the railroad tracks and Hwy. 54 and flows to the northeast. The rest of the site drains to Koppers pond. The pond has an outlet to the south which drains to another pond on residential property across the road. City water is not.available in the area immediately surrounding the site. Residents and business are dependent on private wells for water supply.
NC CERCLA. Unit personnel Pat DeRosa and Mark Durway initiated a site inspection of the Koppers site on December 19, 1986. Since an on-site inspection was postponed awaiting a meeting with Koppers representatives, off-site well sampling was planned to address contaminant migration and potential public health concerns. We arrived at the site at approximately 1000 hours. We drove around the perimeter of Koppers property in order to identify and locate off-site wells previously sampled. Based on previous sampling, topography, and prior contact with off-site well owners, 6 wells were selected for sampling.
We began sampling at 1115 at Triangle Materials approximately .5 miles southeast of the site. This well should serve as a background groundwater sample. We subsequently sampled the residential wells at the homes of James Crowe, William Barbee, George Harding, John Medlin, and Louis Barbee. These wells were purged prior to sampling except where owners cautioned us against running the well dry. Samples were collected for volatile and extractable organics, inorganics, and low concentrations of acid extractable phenolics (i.e. PCP). Samples.were preserved accordingly and submitted to the NC State Laboratory of Public Health for analysis.
On January 7, 1987, we returned to the site to meet with Koppers representative, Mike Dvorsky, and Jim Campbell and ~larty Schlesinger of Keystone Environmental Resources (KER). KER works under contract with Koppers to provide laboratory services. We toured Koppers' portion of the site and obtained background information on the former PCP treatment operations. We also discussed site sampling and cleanup activities which had been conducted at the site to date. Additional sampling data and hydrogeologic information is forthcoming from Koppers and KER.
If you have any questions, please contact me at [phone].
·sincerely,
~Je/vr-
PD/tb/0338b
Pat DeRosa, Waste Management Specialist
CERCLA. Unit
Solid and Hazardous Waste Management Branch Environmental Health Section
N. C. Department of Human Resources
Division of Health Services
. . receiv~~ -~ J / -3 0-&5~ oratory of Public Health
SAMPLEANALYSESREQUESl ~ P.O.Box28047
· · · . ·-·. :-~::-:-. ;306 N. Wilmington Street
Raleigh, 276 I I
~9~'.!2-~~6~0~0~3~2-~e-{)~~3~8~3~--Field Sample Number ~3"---'5"---/-i7f----------
Namc of Site -,,4'--"-"~4/¥1--6L'o~'--'('-;,-'-{4"""'--=-r--'r,""'n_,_
1
_,,C.
0
~#----Site Location ,/l@j 51/'l J:1lot1/l~ilfl/(-,,_ N'(:'
Collected By ~ ~ --'-'3-=8'.=--Date Collected /c2 -[7--f? 6 Time //IS--
Site Number
T ypc of Sample:
Concentrate Comments
Enyonmental
:,,.L__ Groundwater ( 1)
___ Surface Water (2)
__ Soil (3)
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
@ looa9Le /Jhl:. ?<H.lf
__ Other (4)
Extractables
Parameter Results mg/ 1
__ Arsenic
__ Barium
__ Cadmium
__ Chromium
__ Lead
__ Mercury
__ Selenium
__ Silver
----
----
--
Paramei:er Results mg/ 1
_P&T:GC/MS -
_,f___ Acid:B/N Ext. ✓
_TOX
---p{'p' --
MICROBIOLOGY
Parameter
__ (MF) Coliform Colonies/lO0mls
__ (MPN) Coliform Colonies/lO0mls
Dare Received
Reported By
Di•IS 3 1 q I ( R~•vis.:d 7185)
Snli,t and f-fawrdnus \Vaste ( Review 7 /87)
INORGANIC CHEMISTRY
Parameter Results mg/ 1
__ Arsenic
__ Barium
__ Cadmium
__ Chloride
__ Chromium
__ Copper
__ fluoride
__ Iron
__ Lead
__ Manganese
__ Mercury
__ Nitrate.
__ Selenium
ORGANIC CHEMISTRY
Parameter
_EDB
__ PCB'.s
__ Petroleum
__ Endrin
__ Lindane
Results mg/ 1
Parameter
__ Gross Alpha
__ Gross Beta
Total
Parameter Results mg/ 1
__ Silver .
__ Sulfates
__ Zinc
_Ph
__ Conductivity
_ms
_Toe
----
--
----
--
Parameter Results mg/ 1
__ Methoxychlor .
__ T oxaphene
_2,4-D
__ 2,4,5-TP (silvex)
--
RADIOCHEMISTRY
Results PCi/1
'
N. C. Department of Human Resources
Division of Health Services SAMPLE ANALYSES REQUEST
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 2761 I
Site Number 9..2-}) 00 3 2. &-0 3 8 3 Field Sample Number ----''-"]'-'S-,~/-=cf ________ _
Name of Site -l',~-'--""--Fl-¥1'-F,-L-='-C'-~~·9""""-c_=,_.....µ"--n~lc.D=#-_-=.~-=.-=-~~-Site Loca:ion ,llaJ S<f,. ;Jl.,)uz -illi 1( _.,_ UC'
Collected By ~ ./!J.!1:£Lt 3 8'. Date Collected /..2 -I? -R 6 Time I a O Q
Type of Sample:
Concentrate Comments En7onmental
:,L_ Groundwater ( 1)
___ Surface Water (2)
__ Soil (3)
__ Solid (5)
__ Liquid ( 6)
__ Sludge (7)
__ Other (8)
, Tarn e..s Ceo cJJe u-H! P/J
__ Other (4)
INORGANIC CHEMISTRY
Extractable• Total
Parameter Resulto mg/1 Parameter Resulto mg/ 1 Parameter Result• mg/1
__ Arsenic __ Arsenic __ silver
__ Barium __ Barium __ Sulfates
__ Cadmium __ Cadmium __ Zinc
__ Chromium __ Chloride _Ph
__ Lead __ Chromium __ Conductivity
__ Mercury __ Copper _ms
__ Selenium __ Fluoride _TOC
__ Silver __ Iron . --
--__ Lead --
--__ Manganese --
--__ Mercury --
--__ Nitrate --
--__ Selenium --
ORGANIC CHEMISTRY
Parameter Reoults mg/ 1 Parameter Re•ults mg/ 1 Parameter Results mg/ 1
_P&T:GC/MS _EDB __ Methoxychlor
__,.,f_ Acid: BIN Ext. __ PCB'.s __ Toxaphene
_TOX __ Petroleum _2,4-D
--PC'R'
__ Endrin __ 2,4,5-TP (silvex)
--__ Lindane --
MICROBIOLOGY RADIOCHEMISTRY
Parameter Parameter Results PCi/ 1
__ (MF) Coliform Colonies/!O0mls __ Gross Alpha
__ (MPN) Coliform Colonies/!O0mls __ Gross Beta
----
----
I
i
Date Received j d · I 0 • -~G ff, 1L r1 .
Date Reported ___________________ _
Date Extracted ~~~?_· '"-f,_f_,~v~··.·~[~::-_· ___________ _ Date Analyzed ~/._-~i~7--·.,.Y ... 7,',;-r.-/.3..,.iJ~~-------6 '.13403
Reported Oy Lab Number ___________________ _
OHS ) I Gl ( Revi:.ed 7185)
N.~C. Ot:p3rtmem of Human Resources
Division of Ht:alth Services SA1-1PLE ANALYSES REQUEST
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
9...2-6 00 3 2. &-0 3 8 3 Field Sample Number
Raleigh, 27611 3511
Site Number
Nam~ of Site
Collected By
-4L_jy~rFA<:A: rnlc.D·#--'-''-""'----SiteLoca-ioc ,ll«lj sv, ttlt>UZ~i/Jt/(<-A((?
.C£1 ./!.J.'Q£./± 3 8' Date Collected /.,2 -!'7--f? 6 Time 13 f S '
Concentrate Comments
Type of Sample:
~zonmental
Groundwater (I)
___ Surface Water (2)
__ Soil (3)
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
CiJ /JJ, ilia m Bacio ee , i ff o e
__ Other (4)
INORGANIC CHEMISTRY
Extractable• Total
Parameter Results mg/ 1 Parameter Results mg/ l Parameter Results mg/ l
__ Arsenic __ Arsenic __ Silver
--Barium __ Barium __ Sulfates
__ Cadmium __ Cadmium __ Zinc
__ Chromium __ Chloride _Ph
___ Lead __ Chromium __ Conductivity
__ Mercury __ Copper _ms
__ Selenium __ Fluoride _Toe
__ Silver __ Iron . --
--__ Lead --
--__ Manganese --
--__ Mercury --
--__ Nitrate --
--__ Selenium --
ORGANIC CHEMISTRY
Parameter Results mg/ 1 Parameter Results mg/1 Parameter Results mg/ 1
_P&T:GC/MS _EDB __ Methoxychlor
L Acid:B/N Ext. __ PCB's __ T oxaphene
_TOX __ Petroleum _2,4-D
--PCP __ Endrin __ 2,4,5-TP (silvex)
--__ Lindane --
MICROBIOLOGY RADIOCHEMISTRY
Parameter Parameter Results PCi/ I
__ (MF) Coliform Colonies/l00mls __ Gross Alpha
__ (MPN) Coliform Colonies/lOOmls __ Gross Beta
----
----
Date Reported ___________________ _
Date Analyzed -1....f_--'-7_-....JJ...,Y_'J.:....c.,;3c._::i:.:a1fc..· ________ _
Rt."portcd f\y Lab Number 6'':3110,:1
N. C. · Department of Human Resources
Division of Health Services SAMPLE ANALYSES REQUEST
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 2761 I
Site Number _,_9....,!l-=-_,/)"""----=0'--'0"----3"-"'2.=------=<9--0'---"''-'3=-Z--=3"----Field Sample Number ---'3=-'=~"--"J'-Q-· ________ _
NameofSite _,,4-,'-'--'"'.,E.1'3/¥--,r.=.:t:..C.L.{-',&...&L.,-.kld.n~c.-____ Site Location Jim! S'i. trlo«z~1u1l/<. !Ve
Collected By '/4:i-iS;;;;;;, ID# -~3~8'~-Date Collected
I
Jo2-1-i!.. R 6 Time l'f'/S
Type of Sample:
Concentrate Comments En7onmental
..._f_ Groundwater ( 1)
___ Surface Water (2)
__ Soil (3)
__ Solid (S)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
{i) Gecc9e /lorcR,07 u1e I/
__ Other (4)
Extractable&
Parameter Results mg/ 1
__ Arsenic
__ Barium
__ Cadmium
__ Chromium
__ Lead
__ Mercury
__ Selenium
__ Silver
--------
--
·Parameter Results mg/ 1
_P&T:GC/MS
..d-Acid:B/N Ext.
_TOX
--PCP --
MICROBIOLOGY
Parameter
__ (MF) Coliform Colonies/lO0mls
-,.-(MPN) Coliform Colonies/lOOmls
Date Received I ;). · 1 7 -\\a \-0
/1....: -:';.
Date Extracted ;;: -Jt--?h -I;· 5 '
Reported Ely
OHS JIQJ (Re•:i~c-.:17/85)
INORGANIC CHEMISTRY
Total
Parameter Results mg/1 Parameter Results mg/1
__ Arsenic __ silver
__ Barium __ Sulfates
__ Cadmium __ Zinc
__ Chloride _Ph
__ Chromium __ Conductivity
__ Copper _ms
__ Fluoride _TOC
__ Iron --
__ Lead --
__ Manganese --
__ Mercury --
__ Nitrate. --
__ Selenium --
ORGANIC CHEMISTRY
Parameter
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
Results mg/1
Parameter
__ Gross Alpha
__ Gross Beta
Parameter Results mg/ 1
__ Methoxychlor
__ Toxaphene
_2,4-D
__ 2,4,5-TP (silvex)
--
RADIOCHEMISTRY
Results PCi/ 1
Date Reported ----------:--'---------
D I /-7-J'7 ;:3;__0 ate Ana yzed ------=--,~..,-Hl~.e<-------6' 134.05
Lab Number ___________________ _
N. C. Depo.rtment of Hl!man Resollrcc:s
i)ivision of Ht:d!:h Services SAMPLE ANALYSES REQUEST
State Laboratory of Public Heakh
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611
Site Number ,,.9....,.2-=._A._,__,O"--""0'-'3""--'2.""--::::&-0C-""'---'3=:.....:3=--==3"-_-Field Sample Number _· _3__,_S_v_~,1-' ---------
Name of Site ,~~f'l-c4/¥1J=C.'--'L..'L...>-&...,._L..,,,n~c.~---Site Location ,//@fl Si!,, t21.Accz ~1u1!f <-Ye
Collected By -,JJ;fu; jfL)./4 ID# _ _,_3'""-"8',.,___ Date Collected ;?-I.;--_ f? 6 Ti~, /S .:1 ,S'
Type of Sample:
~7onmental
Groundwater (I)
Concentrate
__ Solid (5)
Comments
@ J{)ha tl2edlt'a ul(?lf
·--Su!face Water (2) ___ Liquid (6)
__ Soil (3) __ Sludge (7)
__ Other (4) __ Othet (8)
INORGANIC CHEMISTRY
Extractable•
Parameter Results mg/ 1
I A . 1--rsentc
,--Barium
-·-Cadmium
__ Chromium
____ Lead
__ Mercury
__ Selenium
__ Silver
--
·--
--
--
--
I Pd.rarneter Results mg/ 1 I
_P&T:GC/MS
L Acid:B/N Ext.
_TOX
="P_e,p
MICROBIOLOGY
Parameter
!--(MF) Coliform Colonies/JO0mls
I __ (MFN) Coliform Colonies/!OOmls
1--\-
Repnrt~d 3y
DH:> 3i 111 !Bc.-ised "l/35)
Total
Parameter Results mg/ 1 Parameter Results mg/1
__ Arsenic __ Silver
__ Barium __ Sulfates
__ Cadmium __ Zinc
__ Chloride __ Ph
__ Chromium __ Conductivity
__ Copper _ms
__ Fluoride _Toe
__ Iron --
__ Lead --
__ Manganese --
__ Mercury --
__ Nitrate --
__ Selenium --
ORGANIC CHEMISTRY
Parameter
_EDB
__ PCB'.s
__ Petroleum
__ Endrin
· __ Lindane
Results mg/ 1
Parameter
__ Gross Alpha
__ Gross Beta
Parameter Results mg/ 1
__ Methoxychlor
__ T oxaphene
_2,4-D
__ 2,4,5-TP (silvex)
--
RADIOCHEMISTRY
Results PCi/ 1
Date Reported __________________ _
Date Analyzed _/ __ JI_·_~ J ... -,..· 7_,,...,,(c=-6,-=;,.0-=-~------
h :·,'.}JOG
Lab Number
N.vC. Department of Human Resources
Division of Health Services SAMPLE ANALYSES REQUEST
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Site Number
Name of Site
Collected By
9 k 8 2 <&1-' !L D 00 3 2. &-0 3 3 Field Sample Number ___ __.2""'---'J"-----------
Raleigh, 2 7611
,4:e r /A<!A~ ~Ln1c0# ---'-"-'""'---Site Location ,//alj sv,, 1/Jl,:Juz~i/Jll(..,_ ;1/(" ~ ia'M_,4 38'. Date Collected /,;}, -t? -Ji> 6 Time 17 2-()
Type of Sample:
En7onmental
.!>.L_ Groundwater ( 1)
__ Surface Water (2)
__ Soil (3)
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Ocher (8)
Comments &J Lou.t'.s /Jdrbee (_u.eg_J
INORGANIC CHEMISTRY
Extractables Total
Parameter Results mg/ 1 Parameter Results mg/1 Parameter Results mg/ 1
__ Arsenic __ Arsenic __ Silver
__ Barium __ Barium __ Sulfates
__ Cadmium __ Cadmium __ Zinc
__ Chromium __ Chloride _Ph
_· _Lead __ Chromium __ Conductivity
__ Mercury __ Copper _ms
__ Selenium __ Fluoride _TOC
__ Silver __ Iron --
__ Lead ----
--__ Manganese --
--__ Mercury --
__ Nitrate ----__ Selenium ----
ORGANIC CHEMISTRY
Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ 1
_P&T:GC/MS _EDB _· _ Methoxychlor
£ Acid:B/N Ext. __ PCB's __ Toxaphene
_TOX __ Petroleum _2,4-0
--PCP __ Endrin __ 2,4,5-TP (silvex)
__ Lindane ----
MICROBIOLOGY RADIOCHEMISTRY
Parameter Parameter Results PCi/ 1
__ (MF) Coliform Colonies/lO0mls __ Gross Alpha
__ (MPl,J) Coliform Colonies/lO0mls __ Gross Beta
--------
Date Reported ___________________ _
D A I d I -,Y -Y7 6'J.fl .. ate na yze --"---.-'-_~6~.~. :.-+.J+,,.1_,,0"-'.~_(t--------
Reported Ily Lab Number ___________________ _
DHS JJQJ (R<:vic;ed 7185)
BASE/NEUTRAL ANO ACID
EXTRACTABLES
COIIPOUNO
N-nitrosodirrethvlamine
bis(2-chloroethv11ether
2-chlor~henol
ohenol
l 3-dichlorobenzene
1 4-dichlorobenzene
1.2-<lichlorobenzene
bis(2-chloroi llether
hexachloroethane
N-ni troso-di -n-oroovlamine
nitrobenzene
isonhorone
2-nit~henol
2 4-<lirrethvlohenol
bis(2-chloroethoxvlrrethane
2.4-<lichlo~henol
1 2 4-trichlorobenzene
nanhtha 1 ene
hexachlorobutadiene
4-chloro-<n-cresol
hexachlorocvcl.,..,,.ntadiene
2 4 6-trichlo~henol
2-chloronanhthalene
acenanhthvlene
dirrethvl nhthalate
2.6-dinitrotoluene
acenaohthene
2 4-<linit~henol
2.4-dinitrotoluene
4-n itrooheno 1
fluorene
4-chloroohenvlohenvlether
diethvl ohthalate
4 6-<linitro..o-cresol
diohenvlamine
azobenzene
4-braroohenvlohenvlether
hexachlorobenzene
nontachlorl"V'lohenol
ohenanthrene
anthracene
dibutvl ohthalate
fl uoranthene
STATE LABORATORY Of PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
LAB NO /.0 -fl/ n l '·03<1o < /-03<10 'f /'.03¼° C
FIELD # 3.S-/ 7 3St!I ~S"/9 '1'S..20
TYPE ( I ) ( / ) ( / I r / l
UNITS /2nti) ,on/kQ A,afl) ••"/ko t:,afl) .. a/kq uoi 1) .. a/ko
1~ U-U--iJ---r.,<..-
'I
<o
'0 -s-o
ID
I
J,-
.co
./,
10
I t)
.<; 0
JO
I
A
0/ ' / 1,.-,v ,/
8-FtJ-l.lfe.CL ~ L/f'a.-,.A_
J -Estimated value.
K -Actual value is known to be less than value given.
/-03\/ot,
:.-.,~ I
( / I
--~/l) .. a/kn ..
/
L -Actual value is known to be greater than value given.
U -Material was analyzed for but not detected. The nurt>er
NA -Not analyzed.
is the HinilTUTl Detection Limit.
1/ -Tentative identification.
~/ -On NROC List of Priority Pollutants.
N. C .. V-<.v-0.,-<.on 06 Hea.l:th SVtv-<.c.u
.,-,, 1 r, ? " , C. ,"\ I .f I G' , I _ L ,, ,. _ ..>. ,. •• , , \
/,o3</o 7
'15~.;).
f I l
""/ 1) ,on/ko
LA-
,/
BASE/NEUTRAL AND ACID
EXTRACTABLES
roNPOOND
nvrene
benzidine
butvl benzvl ohthalate
benz!alanthracene
chrvsene
3.3-dichlorobenzidine
bisl2-ethvlhexvllohthalate
di-n-octvl ohthalate
benzo!blfluoranthene
benzo(klfluoranthene
benzo(alnvrene
indeno(l 2.3-cdlnvrene
dibenzo(a.hlanthracene
benzoln h. il....,rvlene
aniline
benzoic acid
benzv 1 a lcoho 1
4-ch 1 oroan i 1 i ne
dibenzofuran
2--<rethvln•nhthalene
2-methvlohenol
4--<rethvlohenol
2-nitroani line
3-nitroani I ine
4-nitroani line
2.4.5-trichloroohenol
STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. OEPARTIIENT OF HUIIAN RESOORCES P.O. BOX 28047 -306 N. WILIIINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEIIICAL ANALYSIS
LAB NO /~o C.:fD~ (,,03<k, 'l /_ a'<<lo <I-/"o3YoS
FIELD# S'S/7 3SI di :::/~ 1 9 ~S-.;:t.D
TYPE ( I l I I ) r I l ( /)
UNITS /.,n/J)un/ko V.,n/l)uo/ka un/ J "l.,n/kn '-•n/ J ). ,nfka
-10 /,L -µ., [,l.-, I -
.:JO
In
' y/
<o ,,/
J O .ri /l)Y
JO {.,I._-
", t)
' /
c;o
I
Ji
10
....,
,") 0
I
I
J/ / , / ,,
m1)L . -
I}-f,.a,d ~ ,<Jt4..,,.J_ µ_J /_e_
J -Estimated value. K -Actual value is known to be less than value given.
/-o3<./olLJ
~s;;z I
( / l
/4n/] "l,n/ka
' '.
.I;
l -Actual value is known to be greater than value given. U -llaterial was analyzed for but not detected. The nurber 1s the llini1TUT1 Detection Limit.
NA -Not analyzed.
1/ -Tentative identification. fl -On NROC List of Priority Pollutants.
N. C. V,i_v-0.,,i_on 06 fleaLth Sv,_v,i_c.v.,
VHS 3068-0 (4/86 Labotz.a.to~y)
✓-o ~s-0 7
~-.:,;;,,.~
( / \
'";,n/Jlun/ka
t.{__
' 1,-
N. C. Department of Human Resources
Division of Health Services SAMPLE ANALYSES REQUEST
State Laboratory of Public Health
P. 0. Box 2804 7
306 N. Wilmington Street
Raleigh, 2 76 l I
Site Number
Name of Site
Collected By
~'l~cJ-~,,_b.,_.Q~D~3~:L~O~f>~3~!?~3~--Field Sample Number -~3-'-='s'--"2,"---3,_ ______ _
&_4f fJe(' ~ ;f ~, w
1
Dc..# :?
0
Site Location //4<Ly ,91 > /JZoc/'1,"; 11,"/fe. if~ .
&_i._/)e_1I.fl,..fA... -2 0... Date Collected· 1/1 -I 7-c:f {, Time /// 5·
Type of Sample:
Environmental
~ Groundwater (1)
___ Surface Water (2)
__ Soil (3)
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
Comments
cD 7c, 'aa7le /)14± ,,t-tlf
INORGANIC CHEMISTRY
Extractables Total
Parameter Results mg/1 Parameter Results mg/ 1 Parameter Results mg/ 1
__ Arsenic __ Arsenic __ Silver
__ Barium __ Barium __ Sulfates ,.
__ Cadmium __ Cadmium __ Zinc
__ Chromium ___ Chloride _Ph
__ Lead __ Chromium __ Conductivity
__ Mercury __ Copper _TDS
__ Selenium __ Fluoride _Toe
__ Silver __ Iron --
--__ Lead --
--__ Manganese --
--__ Mercury --
. __ Nitrate. ----
--__ Selenium --
ORGANIC CHEMISTRY
Parameter Results mg/1 Parameter Results mg/ 1 Parameter Results mg/ 1
_P&T:GC/MS _EDB __ Methoxychlor
__ Acid:B/N Ext. __ PCB'.s __ T oxaphene
_TOX __ Petroleum _2,4-D
7r!.7' ,J--
__ Endrin __ 2,4,S-TP (silvex)
✓ ~2C __ Lindane --
~l. ,,.__ -./J. ~ f} , MfCROBIOLOGY RADIOCHEMISTRY
Parameter Parameter Results PCi/ 1
__ (MF) Coliform Colonies/lOOmls __ Gross Alpha
__ (MPN) Coliform Colonies/lOOmls __ Gross Beta
----
----
Date Received
Z>,l),
Date Extracted ~/.__-LP=~c...-...,f'---'-7---,·•,~··~1~·-__________ _
/. t.~'
Date Reported __________________ _
Date Analyzed ~/_-~(~-~?_7 ---"-,f___,J_L~'.:J~-?,<'.9~-----------
Reported By Lab Number ------'6.,....1~-)3u·LC,}LQ,,,_,,8.,___ ____ _
DHS 31 1)1 (Revised 7/85)
S(ilid and Hazardous Waste (Review 7/87)
N. C. Department of Human Resources
Division of Health Services SAMPLE ANALYSES REQUEST
Srate Laborarory of Public Health
P. 0. Box 28047
306 N. Wilmington Srrect
Raleigh, 27611
9 .,.._ r:> .?-v-7.;,---I Site Number _.L-<.&=-.t.LJ:..J......JOSL.l.OL.,,.,3.,__.,,2=c.J..()L'-Q"---'''-3LJ<LCL..c3"""----Field Sample Number --~.:d=J,:_c:_-4-L----------
Name of Site .kc, 4f':r~, C~, 7:n C Site Loca:ion /tl-<l,9 st:> /llac/'i(IJ///e Ke'.
Collected By /&_f {JpjcoJA._ ID# 3 8' Dace Collected /,::} -I 7-d" c; Time / ,3 /J (J
Type of Sample:
Comments Environmental . Concentrate
~ Groundwater (n ___ Solid (5) {j) .lomea f'.c()111£ 1&1te
___ Surface Water (2) ___ Liquid (6)
__ Soil (3) __ Sludge (7)
__ Ocher (4) __ Ocher (8)
INORGANIC CHEMISTRY
Extractable•
Parameter
__ Arsenic
__ Barium
__ Cadmium
__ Chromium
__ Lead
__ Mercury
__ Selenium
__ Silver
----------
Parameter
_P&T:GC/MS
__ Acid:B/N Ext.
_TOX
Re&ult& mg/ 1
Re&ults mg/ 1
7 / /171' It: b-l't.«l."-.JP cc__---c---
..ri i. " _, -·-_,., -...... - . . ..., , WCROBIOLOGY
Parameter Re&ult& mg/1
__ Arsenic
__ Barium
__ Cadmium
__ Chloride
__ Chromium
__ Copper
__ Fluoride
__ Iron
__ Lead
__ Manganese
__ Mercury
__ Nitrate
__ Selenium
ORGANIC CHEMISTRY
Parameter
_EDB
_PCB's
__ Petroleum
__ Endrin
__ Lindane
Result& mg/1
Total
Parameter
__ Silver
__ Sulfates
__ Zinc
_Ph
__ Conductivity
_TDS
_TOC
--
--
--
--
--
--
Parameter
--Methoxychlor
__ Toxaphene
_2,4-D
--2,4,5-TP (silvex)
RADIOCHEMISTRY
Results mg/ 1
Result& mg/1
Pa.rametcr Parameter Results PCi/ 1
__ (MF) Coliform Colonies/lOOmls
__ (MPN) Coliform Colonies/lO0mls
__ Gross Alpha
__ Gross Beta
Date Recci ved _\l-'2=-::.·...1ic_~,'-' -_,"d,,;""'-?~\'.::!-?b',,'..,__ __ _c ________ Dace Reported __________________ _
' ·B.D.
/-/ 7_. -011-'P. Date Extracted _,_c_c,-=--~'1...CL.J_'-""'~.------------Date Analy:ed ------:-------------A&. ~
Lab Number .) '',J,J.09 Reported By
DHS 31 q I { Re\·ised 7 /85)
' •• '"'--· ,.., ••••• "7 /0"7\
t-,:, C. Department of Human Resources
Divbion of Health Services SAMPLE ANALYSES REQUEST
State Laboratory of Public Health
P. 0. Box 2804 7
306 N. Wilmington Srreet
Site Number
Name of Site
Collected By
Raleigh, 2761 l
__2,,,J_ /) Q Q J .:2 0 {) ,3 8'3 Field Sample Number ~"3~5"_7-,~:5'~--------
./D)_,~9f,:•~~~Ll, w>ID<#_~..t.J--Sitel...ocation/luly ,5'1> t1Zooci1u,lle. ff<!.
£"-;t_/)e/W.14.. 3 g Date Collected /:J -I 7-d' C. Time / ,3 'ti:,
Type of Sample:
Environmental . Concentrate Comments
~ Groundwater {I)
___ Surface Water (2)
__ Soil (3)
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
@ ~ t(,!t(/; 'aq 6ac/4ee 1 <i-f r/f
__ Other (4)
INORGANIC CHEMISTRY
Extractables Total
Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ 1
__ Arsenic __ Arsenic __ Silver
__ Barium __ Barium __ Sulfates
__ Cadmium __ Cadmium __ Zinc
__ Chromium __ Chloride _Ph
____ Lead __ Chromium __ Conductivity
__ Mercury __ Copper __ ms
__ Selenium __ Fluoride _Toe
__ Silver __ Iron --
--__ Lead --
--__ Manganese --
--__ Mercury --
--__ Nitrate --
--__ Selenium --
ORGANIC CHEMISTRY
Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ l
_P&T:GC/MS _EDB __ Methoxychlor
__ Acid:B/N Ext. __ PCB's __ T oxaphene
_TOX __ Petroleum _2,4-D
~,P ,,_.. M,ec
__ Endrin __ 2,4,5-TP (silvex)
✓ __ Lindane --
,,nj,Jl,._,.,..,/,('" /' -.... _,.. , ,I ,fJ , MiCROBIOLOGY RADIOCHEMISTRY
Par2rneter Parameter Results PCi/ I
__ (MF) Coliform Colonies/!00mls __ Gross Alpha
__ (MPN) Coliform Colonies/lO0mls __ Gross Beta
·----
----
Date Reported ___________________ _
Date Analyzed ------7.~""lH-.f--ft--------ti 3410
Rl'porrcd nv --------------------Lab Number
DI-IS 3 I l)\ ( Rt·vis.:d 7 /S5)
1 . "' 1 n • • .•. ""l /C"l\
I
N. C. Department of Human Resources
Division of Health Services SAMPLE ANALYSES REQUEST
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611
Site Number _9~,;L==-LD.J-.. o'-'o..L.L,3.i....:1.=c..e.OL.'-0'-<3-'-'"R'--"3.,__ __ Field Sample Number --~·-3'-'r"".Jc..?ec._~"-----------
Name of Site L~"--YH,"'-~O-~ ,,_
0
__,,_~~-~:;.1.,.,..-_ +T:..,n:...<
1
csDC-# -'-
3
__
0
__ Site Location ffeLy 5-f > /Jla c/'/ I 11t"//e ~◄
Collected By J':ik_.i__fle,lf.L)-L4... _ 0-Date Collected lfJ -1 7-c:f l Time I <f '-IS
Type of Sample:
Environmental . Concentrate
~ Groundwater (1). ___ Solid (5)
Comments
@ Geoo/e /!acd/oy 11Jfl€
___ Surface Water (2) ___ Liquid (6)
__ Soil (3) __ Sludge (7)
__ Other (4) __ Other (8)
· INORGANIC CHEMISTRY
Extractables Total
Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/1
__ Arsenic __ Arsenic __ Silver
__ Barium __ Barium __ Sulfates
__ Cadmium __ Cadmium __ Zinc
__ Chromium __ Chloride _Ph
__ Lead __ Chromium __ Conductivity
__ Mercury __ Copper _ms
__ Selenium __ Fluoride _TOC
__ Silver __ Iron --
__ Lead ----
--__ Manganese --
--__ Mercury --
--__ Nitrate. --
__ Selenium --·--
ORGANIC CHEMISTRY '
Parameter Results mg/ 1 Parameter Results mg/1 Parameter Results mg/ 1
_P&T:GC/MS _EDB __ Methoxychlor
__ Acid:B/N Ext. __ PCB's __ Toxaphene
_TOX __ Petroleum _Z,4-D
Pi!_7' t'.: ~ e C
__ Endrin __ Z,4,5-TP (silvex)
✓ __ Lindane --.A)/,,, __ , .... .,. --. /I , -iJfCROBIOLOGY RADIOCHEMISTRY
Parameter Parameter Results PCi/ 1
__ (MF) Coliform Colonies/lO0mls __ Gross Alpha
__ (MPN) Coliform Colonies/!OOmls __ Gross Beta
--------
'
Date Received \ '2.-I °I · '6-<, 'i-6 Date Reported _________________ _
I g7t,.r ..
Date Extracted-/ .2:· :1{ -P. f·. p..
Reported Ily
DHS 3 I 01 ( Revi!\cd 7185)
•• ,. ' ' '"'·•··· '"·· , •••• ., 1(;>""1\
Date Analy:cd ----~------'---------
Lab Number ____ f;_'._)3_4_1_1 ______ _
N. C. Department of Human Resources
Division of Health Services SAMPLE ANALYSES REQUEST
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611
Site Number ~-lu&=--Lb..J...-'o'-"-'-0,._,,,__,3_.,,2.a,_;...Q!....\Q"'--'3..u..f?L.=3"----Field Sample Number _ _;·3=--5_·-_·2_._7...:...._. _______ _
Name of Site .& 4 oec 5 f'~ '/JJ c Site Loca:ion ,//u1y Si: ., /llac,O./tJ;"//e ~
Collected By s. t:be !?Au ; ID# --'3...,,__,_g',__ Date Collected . If} -L 7-g C. Time l 5 :J ,2
Type of Sample:
Environmental . Concentrate
_.::,.L Groundwater (1). __ Solid (5)
Comments
(i) , lb /211 lhedli a ;,()/ff
___ Surface Water (2) ___ Liquid (6)
__ Soil (3) __ Sludge (7)
__ Other (4) __ Other (8)
INORGANIC CHEMISTRY
Extractable• Total
Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ 1
__ Arsenic __ Arsenic __ Silver
__ Barium __ Barium __ Sulfates
__ Cadmium __ Cadmium __ Zinc
__ Chromium __ Chloride _Ph
__ Lead __ Chromium __ Conductivity
__ Mercury __ Copper __ TDS
__ Selenium __ Fluoride __ TOC
__ Silver __ Iron --
__ Lead ----
--__ Manganese --
--__ Mercury --
__ Nitrate ----__ Selenium ----
ORGANIC CHEMISTRY
Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ 1
_P&T:GC/MS _EDB __ Methoxychlor
__ Acid:B/N Ext. __ PCB's __ Toxaphene
_TOX __ Petroleum _2,4-D
711 ;.z, .;-__ Endrin --2,4,5-TP (silvex)
✓ ~.ec __ Lindane --
f)i..A -_,• ---,.. • ... .i'J , MICROBIOLOGY RADIOCHEMISTRY
Parameter Parameter Results PCi/ I
__ (MF) Coliform Colonies/lOOmls __ Gross Alpha
__ (MPN) Coliform Colonies/l00mls __ Gross Beta
--------
Date Received _\__c?..=c._-..:.1_0..:.)_-'=&,__,\d)'-=''------'--'-------Date Reported __________________ _
Date Extracted .,_/_-..... /...:;2..;c..=--...:fc..'7'--=,"":'-iaf!,--f·_· _________ Date Analy:ed ----c1fj!ac_~~-.➔·,,.,.3h',}'l-_"l1...:,2,.L--------
Reported By __________________ _ Lab Number __________________ _
. .,,_
N, C. Ocpan,m:nt of Human Resources
Divis.ion of Hea.lth Services SAMPLE ANALYSES REQUEST
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611
Sice Number
Name of Sire
Collected By
CJ4 [) 00 3,2.QQ 3f?3 FieldSampleNumber __ ~3=-5.,_-.,_d'--"'6"'---------k91p0<1ri~~J En
1
D<#_-'-"-U--SiteLoca,ion//ulij ,?f, tJlaoCiohl!e /Vr!,
-/:6t-"r_/l£:/Yl-.14... 3 g' Date Collected 1/1 -17-tf'. C. Time / 7 2-0
Type of Sample:
I
Environmental
~ Groundwater (I)
___ Surface Water (2)
__ Soil (3)
__ Other (4)
. Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
___ Other (8)
Comments Ida r 6ee UJf? f J.
INORGANIC CHEMISTRY
Extractables Total
Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ 1
__ Arsenic __ Arsenic __ Silver
__ Barium __ Barium __ Sulfates •
__ Cadmium __ Cadmium __ Zinc
__ Chromium __ Chloride _Ph
__ Lead __ Chromium __ Conductivity
__ Mercury __ Copper _ms
__ Selenium __ Fluoride _TOC
__ Silver __ Iron --
--__ Lead --
--__ Manganese --
--__ Mercury --
--__ Nitrate --
--__ Selenium --
ORGANIC CHEMISTRY
Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ 1
_P&T:GC/MS _EDB __ Methoxychlor
__ Acid:B/N Ext. __ PCB:s __ Toxaphene
_TOX __ Petroleum _2,4-D
7'e_p ti--
__ Endrin --2,4,5-TP (silvex)
✓ i5Yt,~ r __ Lindane --A1i, ... ___ /.',, r-__ ..,._,., .. /1
y MICROBIOLOGY RADIOCHEMISTRY
Par2meter Parameter Results PCi/ 1
__ (MF) Cc,liform Colonies/l00mls __ Gross Alpha
__ (MPN) Coliform Colonies/!00mls __ Gross Beta
--·--
----
Date Reported ___________________ _
Dare Analyzed -----~~-c-,,,-,,...;;-,·:..,':---------6 ;~J413
Rt:port~d Oy Lab Number ___________________ _
[ll!~ J1 1>: /Rt·vi'>cJ 7185)
_ l. n·••••-,r,-.; .... "7 /U-,1
BASE/NEUTRAL AND ACID
EXTRACTABLES
CO!IPOUND
N-nitrosodimethvlamine
bis(2-ehloroethvllether
2-ehloroohenol
ohenol
l 3-dichlorobenzene
1,4-dichlorobenzene
1.2-dichlorobenzene
bisC2-ehloroi llether
hexachloroethane
N-o i troso--di -n...nrnnv l amine
nitrobenzene
i srnhorone
2-oitrnnhenol
2.4-dimethvlohenol
bis(2-ehloroethoxvlmethane
2 4-dichlornnhenol
1.2.4-trichlorobenzene
n>nhthalene
hexachlorobutadiene
4-ehloro-m-cresol
hexachlorocvclnn<>ntadiene
2 4 6-trichlornnhenol
2-ehloron;onhthalene
acen•nhthvlene
dimethyl phthalate
2.6-dinitrotoluene
acen•nhthene
2.4-dinitroohenol
2.4-dinitrotoluene
4-nitrnnhenol
fluorene
4-ehlo=henvlohenvlether
diethvl ohthalate
4. 6-di ni tro-o-creso l
diohenvlamine
azobenzene
4-braooohenv l ohenv l ether
hexachlorobenzene , ,
STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC rnEMICAL ANALYSIS
LAB NO /-o3'IOY /-o3'109 /,,,.,3'//0 /,o3<// I
FIELD # 35" o-< 3 -=J.S.o< <I 3 s-,;, :s-::, ,-o1 /,,,
TYPE ( / ) C I l ( / ) ( / 1
UNITS (un/Uuo/kQ ,-;;n/ 1 h,o/ko l/4n/1} ""/ko v.-;;;/ 1 Ln/ko
o,,ntachlornnhenol \J..--_ ~ /J,t) //,0 < /, /) < /,0
ohenanthrene l
anthracene
dibutvl ohthalate
fl uoranthene
J -Estimated value. 7) /J I,_ '
K -Actual value is known to be less than value given. r'CP 17/{C( '-/ 5 , 5
L -Actual value is known to be greater than value given.
1~03'V/~
"C?J, ol 7
( / 1
..--;,nf1J .. n/ka
< /,0
U -Material was analyzed for but not detected. The nurber
NA -Not analyzed.
is the H_inirrun Detection Umll.
l/ -Tentative identification.
~I -On NROC List of Priority Pollutants.
N. C. D-i.v-u.i-i.on 06 He.a.Uh SVtv-i.c.v.,
Df/S 3068-0 14/86 Labo1ta,l:01tl{)
00 ?U,J
-~J,~Y
( / )
'---;,n/J l,n/ko
<II)
~; Jc!. ~/60 ~r~ {_)..J-(_ 'f-t--.._ . _> /ict o J-l u 1° MN U3
N. C. Dcpa<Cmcn< of H~sou,ccs r ~¥"' •
3
C ..
1
·,a':"'! boratory of Public Hcal,h
Division of Heald, Services SAMPLE ANALYSES ~QI P. o. Box 28047 l 306 N. Wilmington Street
Raleigh, 276 I I
Site Number 9o2 D a O 3 2-Q () 3 <t 3 Field SampleN~b';:\-":=-·::··~64-~~.i...-._L ______ _
Name of Sire -A:.o o,,oec s: Cn ZLI c. Site Location. 1-luJy :r ½ 127,v,(j o,l!c t.J(
Collected By ,&7M e f/o,s I?--' ID# ·38 Dare Collected id-. -/ 7-cf{~ Time ,L.li S:
Type of Sample:
Environmental
_L_ Groundwater ( 1)
___ Surface Water (2)
__ Soil (3)
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
INORGANIC CHEMISTRY
Commcnt6
Extractables Total
Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ 1
__ Arsenic J Arsenic «:.. o. °i, _,_,L Silver <a. o C::
__ Barium ./ Barium ,I}. __ Sulfates
__ Cadmium ,./ Cadmium < c.9· C:':'c."?S-__ Zinc
__ Chromium __ Chloride _Ph
__ Lead ~Chromium -<' ,9. Dl __ Conductivity
__ Mercury __ Copper _TDS
__ Selenium __ fluoride _TOC
__ Silver __ Iron --
.,.L__1.ead < p.&J -----.. -···· __ Manganese --<a,0<2e2;:,, --
--__.,,,L Mercury --
--__ Nitrate --
_.L. Seleniu;., ,::: ,t? oos------
ORGANIC CHEMISTRY
Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/1
_P&T:GC/MS _EDB __ Methoxychlor
__ Acid:B/N Ext. __ PCB's __ Toxaphene
_TOX __ Petroleum . 2,4-D
__ Endrin __ · 2;4,5-TP (silvex) --__ Lindane ----
MICROBIOLOGY RADIOCHEMISTRY
Parameter Parameter Results PCi/ 1
__ (MF) Coliform Colonies/lOOmls __ Gross Alpha
__ (MPN) Coliform Colonies/lOOmls __ Gross Beta
--------
Date Received --------'------Date Reported __ 1'-l· J'-t.._,_l__,l'-'r"--'-2 ______ _ l I
Date Extracted ___________________ Date Analyzed
Reported lly Lab Number U25 ;JCJ DEC 22 Bfi
DHS JI()[ (Rcvi=d 7/85)
S1,li,I ~nd H~ian.ious Wasc<· (Rt".vinv 7/87)
'A~/&; ~r~ v-H·fi--~ :5 . /J'--f o:r
N. C. Dcparun,nr of Human Resources . :·. ·C r D " I ft . ,,---Sca .... ,c_La_bo_to_---...b. Health
Divi>ion ofHcalth_Scrvicea . . .· . SAMPJ-~~~~--· _T __ 28047
n Street
Site Numba ----LZ ... ~.._.D ... · '-'-·o..,_,.o"--3.,_· .... 2.,. .... o ... · ... o ....... .3 .... : .... ~_,3,:: .•. _·. --Field-Sample Number __:,.:::.I~~-~~ba=m.;..,:.:z.:.1,
0
~· _
27
_
6
_
11
:~~ds; c.,· ·2f~:-~· ,l)..,@U/.,·.!<·,,,~;~g;;--'~"-..U_,-· ·_··_\..,~_.•· <.Jo"'·~---· __ 3-· -8---o::·:u::· 'ff% 7!t·~tj!di~"f ~1{;
Type of Sampt;,;°
. _ .. Environmental
. 2 0r:~water ( 1)
~ Su.face Water (2)
·--Soil (3).
--. C>th<r (4)
Concentrate . .-,:•.;:.i. ··r.:::
.. • -·, .. ·.' -·~,-.··:: ..
__ Solid (5) ..
. . --. -. :·-.. , Comments' -:.::( ..
@, Tf>/2~ filecf lt'a ,,oet{f ·',·; .
__ Uquid (6)
__ Sludge (7)
__ Other (8) . .
INORGANIC CHEMISTRY
Extractables Total
Parameter Resultsmg/1 Parameter Results mg/ 1 Parameter
__ Arsenic 'S Ancnic :,;;..C!,'?f :J.Lsilver
__ Barium __ Barium o. __ Sulfates
__ Cadmium ./ Cadmium <:: ,9, oos-__ Zinc
__ Chromium __ Chloride _Ph
__ Lead ~Chromium :S ,p.01 __ Conductivity
__ Mercury _Copper _ms ..
. __ Selenium ... __ Fluoride _Toe
__ Sliver __ Iron "··· ... --... .. -........... . .. . .. --·--...±1.cad· <LJ,025 ----
--__ Manganese --
--.......,L. Mercury -<t2. 'OOo" --
__ Nitrate. --...LSelenium ::;;.Q,00.S --
----
ORGANIC CHEMISTRY
Parameter Results mg/1 Parameter Results mg/1 Parameter . -
_P&T:GC/MS _EOB __ Methoxychlor
_ Acid:B/N Ext. __ PCB's __ Toxaphene
_TOX __ Petroleum _2,4-D -, . __ 2,4,5-TP (silvcx) ----\',/EO ,. .. -· --. ...._ --I -'I,,\
MICROBIOLOGY
'4\ RADlOCHEMISTRY
~
,.
Results mg/1
<o,o5
.
Results mg/1
,.
....
Parameter " !Ail ;J 1(1~. ' ~ lPara~cter Results PCi/ 1
. ;:;
__ ( MF) Coliform Colonies/ I OOmls \ #-Gross Alpha
__ (MPN) Coliform-Colonies/ IOOmls Gross Beta
~ ,, ' •o-------
Date Received ----------'--------Date Reported-~-~-~~----------
Date Extracted _________________ Date Analy::.ed ________________ _
Reported By --------------Lib Number ___ O_2_S_•'J_'J_J_0_E[_?-"-.2-=--86-=------
N. C. Department of Human Resources
Division of Health Services SAMPLE ANALYSES REQUEST
Seate Laboratory of Public Health
P. 0. &, 28047
306 N. Wilmington Street
Raleigh, 27611
Site Number _,_,9.J ............ DoC.-'o'--'-'o"'--3...,__,_2~-->-0-<->-0.,__...3._~"'-"3""-_ Field Sample Number -"3::....?-'--"~'-L/:.,_ ________ _
Collected By
Name of Site ~k'.t~o'H-0~o"'e'-'r......;is:_~C-JJ,_,__r;,,__,LaL'c. ______ Site Location /11,<ly :s :t:
&8 e A>,S e:-ID# 38 Date Collected /ct,. -/7-,?t,
l22c2c11/u,'//,. tJ(:
Time / 'f</.S:-
Type of Sample:
Environmental Concentrate Comments
_L_ Groundwater (1). __ Solid (5)
__ Surface Water (2) __ Liquid (6)
@ fucye I-la cc01\1 (I I/ 1 e
--SoH (3) --Sludge (7)
__ Other (4) __ Other (8)
INORGANIC CHEMISTRY
Extractablea Total
Parameter Reaulu·mg/1 Parameter Rcsulu mg/1 Parameter Reaulumg/1
__ Arsenic ".) Arsenic ~ {2_,~ ....,..Lsnver .............. o.o't:.>
__ Barium __ Barium o. ·, __ Sulfates
__ Cadmium ✓ Cadmium -<v.DOS __ Zinc
__ Chromium __ Chloride _Ph
_Lead ~Chromium -< ,:;7,DJ __ Conductivity
__ Mercury __ Copper _ms
__ Selenium __ Fluoride _TOC
__ Silver __ Iron --
--.,..L_Lcad <." ;},LJ3 --
--__ Manganese --
--.......,(.Mercury <:::: -:2 -<:Joe}?-.. --
--__ Nitrate --
--~ Scleniu;,, ..... z,,oa.< --
ORGANIC CHEMISTRY
Parameter Reaulumg/1 Parameter Re<ults mg/ 1 Parameter Re<ultsmg/1
_P&T:GC/MS _EDB __ Methoxychlor
__ Acid:B/N Ext. __ PCB'.s __ Toxaphene
_TOX __ Petroleum _2,4-D
--"iJM"ifO ~ --2,4,5-TP (silvcx)
---f-}indane -.. ~ --
MICROBIOLOGY
4 RADIOCHEMISTRY ~ .. , . .,
Parameter cl/\ls U 0 .
1:,:1,:_; / ~ Parameter Results PCi/ l
--(MF) Coliform Colonics/!OOmls
. '/ Gross Alpha
~/ --(MPN) Coliform Colonies/lOOmls _J.. ~ __ Gross Beta ~ ...
---lJousw,,,..,,'i..."!]:/
----
Date Reccived ------------------Date Reported ~--~5_-_-_9_,_·~7 ____________ _
Date Extracted------------------Date Analy:ed __________________ _
---------------Lab Number __ ,.l i .. 2~5,_'/._'·~z,-)_,[,..Jt..,C.,_,2...,,.._· .:,::8.,,_6 _____ _
N: C. Dcparrmcnt of Human Resources
Divhion of Hc.alth Services SAMPLE ANALYSES REQUEST
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611
Si1c Number -L9,Q;',1__.D~.Lr~>0"---3"-"2~-.i;.0L'-..0.,__3Lx'"'-=3=---Field Sample Number __,3:c.....;?c......:::f-=3=----------
l?Zc1cN u:l!c ~
Tim~ 13 <fS
Name of Sile . . Ko '3/'PC s: C.a To c,_ Sile J_ocarion . 1/ul ( I :s -st" ,&7Me G{),Srr-ID# 3}? Da1eCollected /d,,. ~7-J'fo Collected By '
Type of Sample:
Environmental
_L_ Groundwater ( 1 ).
Concentrate
__ Solid (5) @aJrl/4'am
Comments
f/arlee... a2£Lf
--Surface Water (2) __ Liquid (6)
__ Soil (3) __ Sludge (7)
__ Other (4) __ Other (8)
INORGANIC CHEMISTRY
Extractablcs Total
Parameter Results mg/1 Parameter Reoults mg/ 1 Parameter Results mg/ 1
__ Arsenic -".'.7Arsenic <.c>, 0/._ _..,__Lsilver <o,o.<::;
__ Barium __ Barium o.a __ Sulfates
__ Cadmium J Cadmium <&,eD5-__ Zinc
___ Chromium __ Chloride _Ph
__ uad ...>.LChromium -< <Y•DL ___ Conductivity
__ Mercury __ Copper _ms
__ Selenium __ Fluoride _TOC
__ Silver __ Iron . ---
.,.L_Lead :5.6'-03 ------
--___ Manganese ---
--.......,I.Mercury -<' '2. ,0 (!_c) tSZ ---
---__ Nitrate ---....L. Sclcniu;.. ::5,l),005 -----
ORGANIC CHEMISTRY
Parameter Results mg/ 1 Parameter Reoults mg/ 1 Parameter Results mg/1
_P&T:GC/MS _EDB ___ Mcthoxychlor
___ Acid:B/N Ext. __ PCB's ___ Toxaphenc
_TOX ___ Petroleum _2,4-D
__ Endrin ___ 2,4,5-TP (silvex) ---
---T ;«;a•l'leO -"' ---.. -/ ..
MICROBIOLOGY I -~\ RADIOCHEMISTRY
Parameter § ;. Parameter Rcsulu PCi/ 1 ' . ,, ,, ..... -.... C -'. . .. ... _.,, z __ (MF) Coliform Colonies/lOOmls 0 .i~ Gross Alpha .. __ (MPN) Coliform Colonies/lOOmls ~~ <fj---Gross Beta
/ -?---~Do,--.,,1/ ----
0:-ite Recci\"ed _________________ _ Date Reported __ /_~.c.-~:..-_-..c;;:..·..c7c__ ___________ _
D:atL" Exlractcd _________________ _ Date Analy:cd _________________ _
R1.:poneJ [\y __________________ _ LaS Number 0259'7 I DEC 22 86
N. C. Department of Human Resources
Di"·ision of Health Service&
t,,U-(. 'f1---.._;' V
SAMPLE ANALYSES REQUEST
Site Numbn-'l~ /) '"/') CJ "3 2-I) (1') ,".3 t 3 Field Sample Number 37 8'2--
State Laboratory of Public Health
-P, 0, Box 28047
306 N, Wilmington Street
Raleigh, 2761 I
Name of Site ~~1qaec s: Ca To c. Site Location llu1y !5¥: m1cNuJ/c /V~
,&roe&2..s~ 38 Rfn Collected By ID# Date Collected L,d-.. -L7-Time /,'l)Q
Type of Sample:
Environmental
_L_ Groundwater ( n Concentrate
__ Solid (5)
Commenu
(j) ( uzmea (!,,-()ut£ ;;,Hj.(l
__ Surface Water (2) __ Liquid (6)
__ Soil (3) __ Sludge (7)
__ Other (4) __ Other (8)
INORGANIC CHEMISTRY
Extractablca Total
Parameter Resulumg/1 Parameter Rcaulumg/1 Parameter Results mg/1
__ Arsenic / Arsenic ;;;,.o,~t. _dsilver <o. o.....,
__ Barium ./ l\:irium o. I __ Sulfates
__ Cadmium J Cadmium ~~«,DS-__ Zinc
__ Chromium __ Chloride _Ph
__ Lead ~Chromium < d',OI __ Conductivity
__ Mercury __ Copper _ms
: __ Selenium __ Fluoride _TOC
__ Silver __ Iron --
. dt.ead -< <9-43 ------__ Manganese --
--~ Mercury -< t} ,ooo 7-. --
--.. __ Nitrate_ --
--_.Lse!enium <. 12,, {)() ~ --
ORGANIC CHEMISTRY
Parameter Results mg/ I Parameter Results mg/1 Parameter Rcaults mg/ I
_P&T:GC/MS _EDB __ Methoxychlor
__ Acid:B/N Ext, __ PCB's __ Toxaphene
_TOX __ Petroleum . _2,4-D
--k:Lil.f!lld~ --2,4,5-TP (silvex)
--/ "--Llndane · --., I· -~
MICROBIOLI 1c:;y '!;. RADIOCHEMISTRY "' -JAi'l Paritmeter -0 •:.: i~ti/ 'i Parameter Results PCi/1
__ (MF) Coliform Colonies/lOOmls ~ _/I __ Gross Alpha = CM,fNl Coliform !=o_l<?nics/lOOmls ~ .. .,~,,o,,, __ Gross Beta ~ ..
, \' --
----
Date Recdved ·_· "----------'--------Date Reported __ ;_· _-_'j~-_-_/_?._7 ___________ _
Da{c E1Ctracted _________________ _ Date Analy:ed _________________ _
Reported fly __________________ _
PHS 3JQ\ (RcviS<"d 7185}
N:-C. Depar,ment of Human Resources
Division of Health Services SAMPLE ANALYSES REQUEST
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 2761 l
Site Number .· 9,,1, D () Q 3 2-D O 3 <I( 3
Na;,,e of Site ~ 0oec S:: Ca Ll C,
Collected By & / 1-t) e A),S e,-ID# 38
Type of Sample:
Environmental
_L_ Groundwater (1)
Concentrate
__ Solid (5)
_·_ Surface Water (2) __ Liquid (6)
__ Soil (3) · __ Sludge (7)
__ Other (4) __ Other (8)
Field Sample Number _..::3=--..±<-:g::....::(:,:__ _________ _
Site Locarion,-+-li.LL(&.,<}Ll?,j.1-,.!5.,_,.tf'c___· ~mu.J.<lu.OLYl1.1j~,llb'LJ/l,,c;.t"..JtJ=e1...._
Date Collected -Ll..cd-.,,,._-_IL..J.7'---'J'J...U{n"---Time / 7 2. D
@ L oui:s
Comments
l5or6ee. we,,e.e
INORGANIC CHEMISTRY
Extractables Total
Parameter Reaults mg/1 Parameter Results mg/I Parameter Results mg/1
__ Arsenic ~Arsenic s.. C2., a L ...i...LSilver <o,o c:
__ Barium __ Barium o.S--__ Sulfates
__ Cadmium ./ Cadmium <' ,9. cJOS-__ Zinc
__ Chromium __ Chloride _Ph
__ uad ....,,L.chromium :$. c?, OL __ Conductivity
__ Mercury __ Copper _ms
__ Selenium __ fluoride _TOC
__ Silver __ Iron --
--d1.cad <,P.03 --
--__ Manganese --
--......,t'. Mercury £:JJ ,oo:) ix --
--__ Nitrate --
--...L Seleniu;,, ,s: 12' E>/).5. --
ORGANIC CHEMISTRY .
Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/1
_P&T:GC/MS _EDB __ Methoxychlor
__ Acid:B/N Ext. __ PCB's __ Toxaphene
_·._··.TOX __ Petroleum _2,4-D
·:.'·:: __ Endrin. ·--·-. ... ·-.: . ·•·.--:=·2,4,5-TP (silvex) --1-__ Lindaoe . ~-----r""i;·;·~ ~Jl -~ ..
MICROBIOLOGY ,:· RADIOCHEMISTRY
I Par2.meter Parameter Results PCi/ 1
f __ (MF) Coliform Colonies/lOOmls (,; : /;
: __ (MPN) Coliform Colonies/lO0mls '•.''..
.
.. '
'"·: . i '--Gross Alpha
; I __ Gross Beta
Date Re..::cived __________________ Date Reported __ J_.-_c:5_·_-__:f>--'7'-------------
Datc: Extrac-tcd __________________ bare Analy:ed __________________ _
P,cporrcd ny Lab Number __ ___,Qd.:s25::+'G'JC'/9c;.,,;:;-. +!iQ[RCC::..<;2;u:i24,81./c6 ___ _
' ,·
1
'
fr--.A~?Je~ /r0-er~cf!~:.;t_ ~ dr0t°s of /:2/Yl 1/CL/~o ~
N. C. Department of Human Resour::ces ... -· ::~ State Laboratory of Public Health
DivisionofHealthService~, -c••;---· S
1
CfE .. NALYSES~. • RW·•· 306 N.~l~n:;;,x07:,~:e;
)J; U C ; Raleigh, 2761 I
Site Number ~'--"""'---",..,_-""\t'-''..<..L":~~.:~~-:~,:J,,',P:::"""---Field Sample Number-~~--~'------------
Name of Site -A4lA:P.~:J~,f.:.;.il!l:.~dc.£L£,.~----Site Location /11,11y st; /Jl()('Y'1'oJ/llc;, /r/ (:
Collected By -+--<-<'-4--_.._~,,._,_~,_,_==--ID# 3,? Date Collected /oJ -I 7 -,J' 6 Time //I)
Type of Sample:
Environmental Concentrate Comments
_d__ Groundwater ( 1) __ Solid (5) {j) Zit'aa ale I
IJ1ai. ,&'. If
__ Surface Water (2)' __ Liquid_(6)
__ Soil (3) __ Sludg~ (7)
__ Other (4) __ Other (8)
INORGANIC CHEMISTRY
Extractable• Total
Parameter Results mg/ 1 Parameter · . -Results mg/ 1 Parameter Results mg/ 1
__ Arsenic __ Arsenic __ Silver
__ Barium __ Barium __ Sulfates
__ Cadmium· __ Cadmium __ Zinc
__ Chromium __ Chloride _Ph
__ Lead __ Chromium __ Conductivity
__ Mercury __ Copper _TDS
__ Selenium __ Fluoride _Toe
__ Silver __ lron --
--__ Lead --
--__ Manganese --
--__ Mercury --
--__ Nitrate --
--__ Selenium --
•
ORGANIC CHEMISTRY
Parameter Results mg/1 Parameter Results mg/ 1 Parameter Results mg/ 1
1--\L. P&T:GC/MS _EDB __ Methoxychlor
__ Acid:B/N Ext. __ PCB's __ T oxaphene
_TOX __ Petroleum _2,4-D
--__ Endrin __ 2,4,5-TP (silvex)
--l, ( t"l LrDtJ.1/ e':f-4 er. · __ Lindane --;-; .
MICROBIOLOGY RADIOCHEMISTRY
Parameter Parameter Results PCi/ 1
__ (MF) Coliform Colonies/l00mls
__ (MPN) Coliform Colonies/l00mls
__ Gross Alpha
__ Gross Beta
D R d I"\ I q a t-C--.. 1/.1 y/h' :7_
ate ccei ve .-"t.,;d-ec,_--1._L·_,,_6Vl_:::___:_ru_:-L_ __ -'--------Date Reported -.~, ----'7'1-'--'--'-'C/'--'-/-_______ _ rr , __
Date Extracted -----------~-------Date Analyzed -~'~;~t_-~;,,~j _-~1.,,✓~~(•'c-~ ~\~~,!-1
3!:z lc.•,9=,--·c=~--------
Reported fly --,.L/4~;,.,#~, ,/2_.6_-,,_~.L?_,-_.,:;, ___ :,_/L_L_f_,,_:CL_' ✓~/_1
_______ Lab Number ___________ u ________ _
DI-IS 3191 (Rt·viscd 7/85)
S(1!id :ind Hazardous \Vaste (Review 7/87)
;It: J:-1 /17(> le.a /.reµ,_,,-~ ~ "-ft_ -f cf r0 jJ s of /.J In #C:i:/-1' 0 IX{
N. C: Department of Human Resources State Laboratory of Public Health
Division of Health Services SAMPLE ANALYSES REQUEST P. o. Box 28047
Site Number 9.2 D l)Q 3 2. .9--0 3 8'..3
Name of Site ,J1..,117ec 5: f:n; In C.
Collected By fZ :C /)-e /2.tJ S: °= ID# ,3/?
Type of Sample:
Environmental
306 N. \X1ilmington Street
Raleigh, 27611
Field Sample Number
Site Loca;-ion tf1,t1y S si; /JJc,u,,' aJ/// <;, /r/ (:_
Date Collected /oJ-/ 7 -J' 6 Time /,3 DO
Comtnents
_L,__ Groundwater ( 1)
Concentrate
__ Solid (5) (VI Z102e.s &a,,ie ,ue ee
__ Surface Water (2) ___ Liquid (6)
__ Soil (3) __ Sludge (7)
___ Other ( 4) __ Other (8)
INORGANIC CHEMISTRY
Excractables Total
Parameter Resu I ts mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ 1
__ Arsenic __ Arsenic __ silver
__ Barium __ Barium __ Sulfates
__ Cadmium __ Cadmium --Zinc
__ Chromium __ Chloride _Ph
__ Lead __ Chromium __ Conductivity
__ Mercury __ Copper _ms
__ Selenium __ Fluoride _TOC
__ Silver __ Iron --
--__ Lead --
--__ Manganese --
--__ Mercury --
--__ Nitrate --
--__ Selenium --•
ORGANIC CHEMISTRY
Parameter Results mg/ 1
I ..I.L.. P& T:GC/MS
__ Acid:B/N Ext.
_TOX
--
--I.[() Lro/2,.,/_e 'M ec ;-I
MICROBIOLOGY
Parameter
__ (MF) Coliform Colonies/!O0mls
__ (MPN) Coliform Colonies/!00mls
Parameter
_EDB
__ PCB'.s
__ Petroleum
__ Endrin
· __ Lindane
Date Extracted _________________ _
Reported Ily
[)H~ J\<_ll (R,:viscJ 7185)
Results mg/ I
Paran1eter
__ Gross Alpha
__ Gross Beta
Parameter Results mg/1
__ Methoxychlor
__ Toxaphene
_2,4-D
--2,4,5-TP (silvex)
--
RADIOCHEMISTRY
Results PCi/1
Date Reported _________________ _
Date Analy:ed ------,..-,.-,..-..=:=--------6 ·: ',3397
Lab Number ----------------·---
A-' J;,'>J?le.a /reµ:_,~ c,u-f"ft_ ~ dr0jJS of /.J/12 #C.i'./-10 ~
N.-C. Oepanment of Human Resources State Laboratory of Public Health
Division of Healrl, Services SAMPLE AN AL YSES REQUEST P. o. Box 2804 7
Site Number 9.2-/) QO 3 J.. fHJ 3 8'. 3
Name of Site ,J-hrf;P ('CS f:n , .Zn C:::...
Collected By Ht ;f: /) ,e /2tJ S °= ID# 3/:(
Type of Sample:
Environmental
L Groundwater (I)
Concentrate
__ Solid (5)
__ Surface Water (2) ___ Liquid (6)
__ Soil (3) __ Sludge (7)
__ Other (4) __ Other (8)
306 N. Wilmington Street
Raleigh, 2761 I
Field Sample Number -~3'""-""5"'-';'-"3:::,_ ___________ _
Site Loca:iop /11,t '5' , 5 S-:: ;Jlllrr, 'ah lie;, /t/ C.
Date Collected /,;J-/ 7 -d' 6 Time I, 3 'i:S::-
Comments
® /));l/2 cun Aa che e , m I(!
INORGANIC CHEMISTRY
Extractables Total
Parameter Results mg/ I Parameter Results mg/ I Parameter Results mg/ I
--Arsenic __ Arsenic __ Silver
__ Barium __ Barium __ Sulfates
__ Cadmium __ Cadmium __ Zinc
__ Chroil.1iuni. __ Chloride _Ph
__ Lead __ Chromium __ Conductivity
__ Mercury __ Copper _TDS
__ Se!t:nium __ fluoride _TOC
__ Silver __ Iron --
--__ Lead --
--__ Manganese --
--__ Mercury --
--__ Nitrate --
--__ Selenium --
•
ORGANIC CHEMISTRY
Parameter Results mg/ I Parameter Resu Its mg/ 1 Parameter Results mg/ l
;dP&T:GC/MS _EDB __ Methoxychlor
__ Acid:B/N Ext. __ PCB's __ T oxaphene
_TQX __ Petroleum _2,4-D
__ Endrin __ 2,4,5-TP (silvex)
_ ~12_jjl.e'ttier:. __ Lindane --
MICROBIOLOGY RADIOCHEMISTRY
Parameter Parameter Results PCi/ I
__ (!\ff) Coliform Colonies/!O0mls __ Gross Alpha
__ (MPN) Coliform Colonies/l00mls __ Gross Beta
----
----
Date Reported __________________ _
l).:i.r;._· Extr~cted __________________ Date Analyzed --------,,...-c,.,,,...,..,.,,...,-------6: ,a398
Reported Ily Lab Number
fll·l~ .l 1 •JI ( R,.-·,·i~c•d 7185)
. .. . •··• -,,.....,,
of /.2 m #'C.JZ/.Y tJ ~
N. C. Department of Human Resources
Division of Health Scr..-iccs SAMPLE ANALYSES REQUEST
State Laboratory of Public H1:alch
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 2 7611
Sire Number 9.2 A IJQ 3 ,')__ ()-{) 3 8' .3
Name of Site ,di,/;:f2ec' 'f C-0) 1;n c.,,
Collected By a /: /)-e /2..tJ S: t'.L ID# 3/?
Type of Sample:
Environmental Concentrate
-.J..L_ Groundwater ( 1) __ Solid (5)
___ Surface Water (2) ___ Liquid (6)
__ Soil (3) __ Sludge (7)
--. Other (4) __ Other (8)
Field Sample Number __ 3=:-5=• ~'--1_,t/ ___________ _
Site Loca;ion //1,1 'f ,5~ ll211U't'oJ///c;, /t/ C _
DateCollected /cJ-/ 7 J'6 Time li'-15
Comments
@ Oeocye llocdiar "te..l(
INORGANIC CHEMISTRY
Extractable•
Parameter Re•ult• mg/ l
__ Arsenic
__ Barium
__ Cadmium
__ Chromium
___ Lead
1--Mercurv
__ Selenium
__ Silver
--
·---
--
--
Parameter Remits mg/1
i.d..P&T:GC/MS
__ Acid:8/N Ext.
_TOX
--
--l, [CJ£r0f2-1/ e'Uter. ;-~
MICROBIOLOGY
Parameter
__ (MF) Coliform Colonies/I00mls
__ (MPN) Coliform Colonies/!O0mls
Dare Received /J· l')-f{,, uiJ
Parameter Resulto mg/ 1
__ Arsenic
__ Barium
__ Cadmium
__ Chloride
__ Chromium
__ Copper
__ Fluoride
__ lron
__ Lead
__ Manganese
__ Mercury
__ Nitrate
__ Selenium
•
ORGANIC CHEMISTRY
Parameter
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
Resulto mg/ 1
Parameter
__ Gross Alpha
__ Gross Beta
Total
Parameter Resulto mg/ 1
__ Silver
__ Sulfates
__ Zinc
__ Ph
__ Conductivity
__ TDS
_TOC
--
--
--
----
--
.
Parameter Results mg/1
__ Methoxychlor
__ T oxaphene
_2,4-D
__ 2,4,5-TP (silvex)
--
RADIOCHEMISTRY
Results PCi/ 1
Date Reporred __________________ _
Rc:port,.:d By ___________________ Lab Number
tr: . Az,,-1f>1e.:; /Jre,:i,erve_d] c,u-t"-ft_ -f cf---o;;s uf 1.2m 11c2../-'!o ~
N.-C. Department of Human Resources State Laboratory of Public Health
Divi,ion of Health Services SAMPLE AN AL YSES REQUEST P. o. Box 28047
Sire Number 9.2 b l)Q 3 :L .9-{) 3 8'. 3
Name of Sire ,Ji,/tOfc 5:: Cn 7 ,In <--
Collected By /?:_, ;C /) ,e /(.I) .S: 6= IO# 3/?
Type of Sample:
Environmental
L Groundwater ( 1)
___ Surface Water (2)
__ Soil (3)
--. Other (4)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
306 N. Wilmington Street
Raleigh, 2761 I
Field Sample Number------------------
Site Loca~ion /11,r/f 1 5 t; $11/1/'/ CiU '/Jc;, /r/ (:
Date Collected /oJ -I 7 -,J' 6 Time /.5' ,)_ S:
Comments
r£) 1 To/20 (}Jedi, ·a u&fR
INORGANIC CHEMISTRY
I Extractable• Total
Parameter Results mg/ l Parameter Results mg/1 Parameter Results mg/ l
__ Arsenic __ Arsenic __ silver
!--Barium __ Barium __ Sulfates
__ Cadmium __ Cadmium __ Zinc
__ Chromium __ Chloride _Ph
___ Lead __ Chromium __ Conductivity
__ Mercury __ Copper _TDS
__ Sc!t"nium __ Fluoride _TOC
__ Silver __ Iron --
--__ Lead --
---__ Manganese --
--__ Mercury --
--__ Nitrate --
--__ Selenium --
•
ORGANIC CHEMISTRY
Parameter Results mg/ l
: ~ P& T:GC/MS
__ Acid:B/N Ext.
_TOX
_ ./..liltCf;A,le 'Ht ec f '
MICROBIOLOGY
Par2.mcter
: __ (MF) Coliform Colonies/lO0mls
__ (MPN) Coliform Colonies/lO0mls
Parameter
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
Date E),·tractcd __________________ _
Results mg/ l
Parameter
--Gross Alpha
__ Gross Beta
Parameter Results mg/1
__ Methoxychlor
__ Toxaphene
_2,4-D
__ 2,4,5,TP (silvex)
--
RADIOCHEMISTRY
Results PCi/ l
Dace Reported ___________________ _
Date Analyzed ---------,,-..---,-,,a-,~~--------
RcportcJ By ------·--------------Lab Number
6: iJ,:100
l )JI~ 11 (I I ! Rcvi.~e,l :' .'85)
-, u --,, J,_,., ,s,•~,·~ n;-~.,; .. ,.. 7 /H7\
fi:t.1'>1(>/&, /r0er~ (/.,'-{'-ft_ -/ dr0,PS of /,2()2 /ICJ!../.i/0 nr..(
N. c:·Department of Human Resources
Division of Health Services SAMPLE ANALYSES REQUEST
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 2761 I
Site Number _,_9,...,:2,=-_./)....,__.,,Q""-Q'"'---',3..J....e,2_=->()-{)<-->-"--'-,3,._._.8'--'.3=---Field Sample Number --·3__.r~/_{.,, _________ _
Name of Site ~,,M-,,._..,_.,"'P=,Lf=c.....,_s:_~(' .. -12~,...-z=11'-'--'<--------Site Loca,ion .#uty ,)r; $(lcr/ct!J lie;,/,/(:_
i?,; I: /)-e 12A SI& IO# 3,? Date Collected /ol -/ 7 -J" 6 Time / '7 2-() Collected By
Type of Sample:
Concentrate Comments Environmental
_L_ Groundwater (1) __ Solid (5) @) Lo LU. s i3o.r6ee.. well
___ Surface Water (2) ___ Liquid (6)
__ Soil (3) __ Sludge (7)
___ Other (4) __ Other (8)
INORGANIC CHEMISTRY
Extractable•
Parameter Results mg/ 1
__ Arsenic
__ Barium
__ Cadmium
__ Chromium
___ Lead
__ Mercury
__ Selenium
__ Silver
--------
--
Parameter Results mg/ 1
..v(___p&T:GC/MS
__ Acid:B/N Ext.
_TOX
--
--L, ({JLrD,')-yl "':/::ttec. ,--.
MICROBIOLOGY
Parameter
__ (MF) Coliform Colonies/lOOmls
__ ( MPN) Coliform Colonies/ lOOmls
Parameter Results mg/ 1
__ Arsenic
__ Barium
__ Cadmium
__ Chloride
__ Chromium
__ Copper
__ Fluoride
__ Iron
__ Lead
__ Manganese
__ Mercury
__ Nitrate
__ Selenium
•
ORGANIC CHEMISTRY
Parameter
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
Results mg/ 1
Parameter
--Gross Alpha
__ Gross Beta
Total
Parameter Results mg/ 1
__ Silver
__ Sulfates
__ Zinc
_Ph
__ Conductivity
_TDS
_TOC
--
--
--
--
--
--
Parameter Results mg/1
__ Methoxychlor
__ T oxaphene
_2,4-D
--2,4,5-TP (silvex)
--
RADIOCHEMISTRY
Results PCi/ 1
/c9 1n1 -g r-!)' Date Received ~---~-'~\o~~=-~----------Date Reported _________________ _
Date Extracted __________________ Date Analy:ed _________________ _
Reported By ___________________ Lab Number 6034-01
DHS°J191 (Revised 7/85)
~,,li,I :>n,l H'l::irdous \VaHc (Re,•iew 7187)
N. C. DEPARTMENT OF HUMAN RESOURCES
DIVISION OF HEALTH SERVICES
SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Chain of Custody Record
Hazardous Waste Materials
Location of Sampling: Generator __ Transporter __ Treatment Facility
__ Storage Facility Disposal Facility Landfill
,/Other: t2.U:nd2~v!L. q.e-a,c ~ccfl!-t) ML 7 ~ J
Company's Name 7/-✓c[&I<?.., ma :lfoJ5 Telephone( ___ .) _______ _
Address ,itz,✓J, ~: £b ,ff~Z> /JJoca,'011/l-e,/ /,/{:.
Collector's Name. i-ii4~ Teleyhone(9-/'.f) J3]-;;zl{)/
signature -
Date Sampled . ,c2/,> 7,/?£ Time Sampled ,l,I ;::, dZ?J
Type of Process Generating Waste -------------------------
Field Information
Field Sample No. 35 I /
Chain of Possession:
1. f,/) ~~
signature inclusive dates
2. /lt-.JJt.~
3.
signature title inclusive
Results reported
signature title date
Instructions: Complete all applicable information including signatures, and
submit.with·analysis request forms.
dates
N. C. DEPARTI!ENT OF HUMAN RESOURCES
DIVISION OF HEALTH SERVICES
SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Chain of Custody Record
Hazardous Waste Materials
CJtj J-vQ tA.J-{.-&
j<c.wp ✓:.r-(!o I r 11 c..
9 c9 b cm 3 2., ((Q 3 J' 3
Location of Sampling: Generator __ Transporter __ Treatment Facilit:
__ Storage Facility __ Disposal Facility __ Landfill
_K_Other: ;fJo ·c1 w £8/2-a b ufr;ql« '=4, a:,,,le--uHIR r ccJ 1
Company's Name facn:e-o (}41,µ.g, CGddl.RH-f Telephone(£ ) _______ _
Address /2'/ay 5 ¥ : moca,1 II rll<
Collector's Name ,3~~
signature
Date Sampled · /ol-1 7 -f G Time Sampled:._--,,,'-/-'c'-1"-. c✓O~a::..._ __ _
Type of Process Generating Waste. _______________________ _
V
Field Information
·Field Sample No. 3 5 / ?-3S:tK 3SJ'-/:
Chain of Possession:
1 .. ~/ul/11:
signature
title -inclusive dates
3.
signature title inclusive dates
Results reported
signature title date
Instructions: Complete all applicable information including signatures, and
submit with ·Bnalysis request forms.
Location of Sampling:
N. C. DEPARTMENT OF HUMAN RESOURCES
DIVISION OF HEALTH SERVICES
SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Chain of Custody Record
Hazardous Waste Materials
Generator __ Transporter
vJJf /~ v-J.-U!,~
;;,'7"J2,a 6 1 .L;?e,
5'cx i) tD J U/D J cf _3
__ Treatment Facilit:
Storage Facility Disposal Facilit:y __ Landfill
X Other: ltt( -d7ll :;=;?:ztfe, (it-cl/
Company's Name
. . Zl(T f/ ,r/cfo,6e-R-/2e (Z?Jl QI~ Telephone(. __ ) ______ _
Collector's Name,~-+--'~::1,_-~=-~.l.La::;__ ___ Tele_phone( 9/f ) 7-3 ?----1/'tP (
Time Sampled,_'1-/_¥ _ __,.,_J:_· .,t.,6~1/YJ-L_
signature
Date Sampled /] ~ I 7 -£,6
Type of Process Generating ·waste. ________________________ _
Field Information
-Field Sample No. 35 / 3 3S!9 35J,5;
Chain of Possession:
/2--1 7-<f(,
t:itle inclusive dates
/d-/ 7~ I 2--✓'1-<f'{,
signature inclusive dates
3.
signature title 'inclusive dates
Results reported
signature title date
Instructions: Complete all applicable information including signatures, and
submit with'2nalysis request forms.
N. C. DEPARTMENT OF HUMAN RESOURCES
DIVISION OF HEALTH SERVICES
SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Chain of Custody Record
Hazardous Waste Materials
¾f clvl2~
/!o/f ;,,✓ <-0 1.)J (_
p,2 /) (JV 3 2-U"O 3.f.3
Location of Sampling: Generator __ Transporter __ Treatment Facilit~
__ Storage Facility __ Disposal Facility __ Landfill
. . _L Other: ~ .t,.11£ 1 f 1°'/' L aLi J ,'11 ✓,,,..., fd1(p-V S
Company's Name ,/l2r, fX-tlJt? ,NP~&P;Telephone( ). _______ _
Address /?Jt CA I ice/.-(f l; t ;;__ th,>< I,{ 112 ,, ca c VI //e, . I -. ;VJ l£ /2.o,CIJ 'rele;hone( f11) 733-i?-cfO/
7 signature
Collector's Name
Date Sampled, _ ___,.,1'-'.;J""--__,,/:...7-1----cf""-. _.f;z.._' ______ _;Time Sampled:.......(Y~_Ll_r__,!L-P,_,1/}1~--,
Type of Process Generating Waste ·-----------------------
. Field Information
Field Sample No. 3 S' / 'f
Chain of Possession:
1. ;z-; 7-FC
sign ure title inclusive dates
2. ~&~1/:1...::/"---,~,(\_..4:"",-,"-/4..:....~.:....6 ~-==-· ___ U/,z~ Wldfacd~-1 Z--r7-J'6 ::::::::i
' signature ' title/ inclusive datj!S~ . . 1.2-1'1-pr:, .
c_··1" J,,, .· ~,,--1)-/lr/<l.~-.. --
title inclusive dates
Results reported
signature title· date
Instructions: Complete all applicable information including signatures, and
submit ~ith·~nalysis request forms.
N. C. DEPARTMENT OF HUMAN RESOURCES
DIVISION OF HEALTH SERVICES
SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Chain of Custody Record
Hazardous Waste Materials
. Location of Sampling: Generator __ Transporter __ Treatment Facilit~
__ Storage Facility __ Disposal Facility __ Landfill
...);,__Other: <'V'··/,?, f; c,//" hQ y , . t,cf " Yll N -"-c Ko/ /.>ff 5 a £?c I ~• /
Company 1 s Name ()? r-.
' ~IA-d, o ;1]r:, .,{/ ID Cc':U cflp,"l'-Telephone(. ___ .) _______ _
Address µ-:l
1 l3=, 1 r' ,L22u,,,-.;J,,,•;Jlc, 1if ('._
Collector's Name._---,,)'.c.,./_./C::wl""L'---t'.',,1f..a..'_./4:...:1:c...:-Pc..~;::;.:: ____ Tele_phone('i/7 ) ? 31-2.{:Ci /
' signature
.? ·2._o /) Date Sampled. ___ /<....:.:;,;),__-...1./c.......,.7_-....c-f'"--"C'-. _______ _;Time Sampled __ -'-.2"----~.;..//......L.f?2·~-
Type of Process ·Generating.Waste ·-----------------------y
Field Information
·Field Sample No. ]5!5' .3SJ.,/
Chain of Possession:
1.
2.
3.
signature
Results reported
signature
title
title
title
/J.·/?-)'.(
inclusive dates
/Z -/ 7-J'6 ,..../2-/9-tf'(,
inclusive dates
inclusive dates
date
Instructions: Complete all applicable information including signatures, and
submit.with ·2nalysis request forms.
, .. Location of Sampling:
N. C. DEPARTMENT OF HUMAN RESOURCES
DIVISION OF HEALTH SERVICES
SOLID AND HAZARDOUS WASTE MANAGEMENT.BRANCH
Chain of Custody Record
Hazardous Waste Materials
Generator __ Transporter __ Treatment Facilit]
__ Storage Facility __ Disposal Facility __ Landfill
. ..L__Other: /Jr I 1/a& <t¾ -,{J;Q, d// ab DJ 1!41hr cA£<d ~ VU I
Company's Name · t-<9-:Gti,'r Aar/2-ee ,·Cf,ui:ieY&:Telephone( ) _______ _
Address Rf: d2 t2J//Cct >u c /I e..., NC:
7 . '
Collector's Name . &r: !Je e{ ,(),;"J-1 Tele_phone ( 91 9 ) 13 j -21' tJ /
signature
Date Sampled:.._ __ ,._/_,.d<L..;.-_,f'.-/-1-7:.._-'-'-d'.._.~~-------'Time Sampled / ;1: 2<J
Type of Process Generating ·waste. _______________________ _
y
. Field Information
·Field Sample No. 35 /(o Z3522-,3,Sa&
1.
Chain of Possession:
__,µ..../22-..;.;::" =---..c.-/4e~tf.l."1.'-(,"-"-'..>./.L.L.2c_.....,.· u.~~ /!&m_ lc/2e.c ~ signature ~ title Y /oid--°} / Z.,7'~ -r?c
inclusive dates
2.
signature title 7 intlusive dates
3.
signature title inclusive dates
Results reported
signature date
Instructions: Complete all applicable information including signatures, and
submit.with ·2nalysis request forms.
. .
STATE LABOAATORY Of PUBLIC HEALTH
DIVISION Of HEALTH SERVICES, N.C. OEPAATNENT Of lfJI\AN RESOJRCES
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 21611
ORGAHIC O!EMICAL ANALYSIS
PURGEABLE aJIIPOJNOS LAB NO /iJIJ 2,}_?,-J /11 /o{i._;; ~,c·1 7 In/' A O\C(0 / ... J-J,~3(t<1
FIELD I
TYPE .t:1. ) ( I l I I I . ( I j aJIIPOJND f.,n/1 ~,n/ko f.,n/lJun/ka (ua/1 J°un/ka ,'i;o/ I/ un/ka UNITS
/l' -{_; __ '------,. -, ~, ch lorcrrethane
braranethane I,,
dichlorodifluoromethane _?. .)
vin"l chloride Jd ;
ch 1 oroethane j i:;
oethvlene chloride 7
trich lorofluoromethane ;2 u
ethene-11--dichloro 5
ethane 1 1--d i ch 1 oro-
1 2-trans--dichloroethene
chlorofona
ethane 1 2--dichloro-
ethane 1 1.1-trichloro-
carbontetrachloride
brooodich loromethane
~-·ne 1 2--d i ch I oro---
L 3--trans--dich lo, !
trichloroethvlene ;
chlorodibrononethane i ' benzene i
ethane 1 I 2-trichloro-1 I
I 3--cis--dichlo, '!J
2-ehloroethvl vi=l ether lo
braroform ,
ethane 1 1.2.2-tetrachloro-
ethene. tetrach Jara---
toluene
chlorobenzeoe I
ethvlbenzene 'JI I ,7 !/ ,/
acetone ID c, ' [A__ L,o.____
2--butdnone /0 I
cart>ondisul fide s
2--hexanone I"
4--mlt""l-2 ~t.,none /iJ
st·-L,--
vinvl acetdte F
o-xvleoe ~-\,_I ,/ / . ,
!
.(-' .:.1 1, "'• ~ I /,, •--; {.' h,'J •''J/""'" .~ p • --i -r'.=·; r-(_L/ (--_)
I ✓ I
J -Estimated value.
l -Actual value is known to be less than value given.
/() /) l;._"31-k) (')
(--1. l
( un/1) .. n/kn
IA-
-,/
k_
,·
( )
L -Actual value· is known to be greater than value given.
U -llaterial w.,s an.,Jyzed for but not detected. The numer is the llininun Detection Limit. NA -Not an.,Jyzed.
I/ -Tentative identification.
~/ -On NROC List of Priority Pollutants.
N.C. Division of llcalth Services
OHS '3068-0 (4/86 Laboratory)
(()u.3 L.]7, I
__ ( i
.. n/ J\ .. n/ko
~
,
. '
/
I
al 5/1qft f-