NCD003188844_19901011_Carolina Transformer_FRBCERCLA RI_Rem Invest - Oct 1990 Phase 4 Off-Site Soil Sampling-OCR

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4WD-NSRB
MEMORANDUM
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
REGION IV
345 COURTLAND STREET. N.E.
ATLANTA, GEORGIA 30365
Date: October 11, 1990
From: Michael Townsend
Remedial Project Manager
To: Jack Butler
Environmental Engineer
Superfund Branch
In case you were not aware, I have replaced Michelle Glenn as the
project manager for the Carolina Transformer Site. I envision there
won't be any further changes in site assignments, and I'll be on the
job for a while.
Enclosed are a couple of things. One is the Draft Risk Assessment
and the other is the subsequent data collect to determine the extent
of contamination. It would be greatly appreciated if you could
review the Risk Assessment and forward your comments to me by the
26th of October. If you have any question or comments concerning the
additional data, forward them to me as soon as possible.
If you need my assistance on anything don't hesitate to contact me.
Thank you for your cooperation.
cc: William Meyer
Printed on Recycled Paper
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MEMORANDUM
DATE:
SUBJECT:
FROM:
TO:
THRU:
U. S. ENVIRONMENTAL PROTECTION AGENCY
REGION IV, ATHENS, GEORGIA
OCT O 9 1990
Phase 4, Remedial Investigation Report for the Carolina Transformer
Site, Fayetteville, North Carolina; ESD Project No. 90-785
;\ \t)
Dan Thoman, Regional Expert -~C""1wi.
Hazardous Waste Section
Environmental Compliance Branch
Environmental Services Division
Michael Townsend
NC Remedial Section
North Superfund Remedial Branch
Waste Management Division
William R. Bokey, Chief
Hazardous Waste Section
Environmental Compliance Branch
Environmental Services Division
Attached is the Draft Phase 4, Remedial Investigation Report for the above
mentioned site. Please review and provide comments.
If you have any questions, please call me at FTS 250-3172.
Attachment
cc: Finger/Wright
Bokey/Hall
Knight
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REMEDIAL INVESTIGATION REPORT
PHASE 4
OFF-SITE SOIL SAMPLING
CAROLINA TRANSFORMER SITE
FAYETTEVILLE, NORTH CAROLINA
by
DANIEL THOMAN
U. S. ENVIRONMENTAL PROTECTION AGENCY
REGION IV
ENVIRONMENTAL SERVICES DIVISION
ENVIRONMENTAL COMPLIANCE BRANCH
HAZARDOUS WASTE SECTION
October 1990
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EXECUTIVE SUMMARY
A Remedial Investigation (RI) was conducted at the Carolina Transformer site in
.Fayetteville, North Carolina, by the US Environmental Protection Agency (EPA),
Region IV, Environmental Services Division, Hazardous Waste Section (HWS). The
RI, conducted in four phases, was performed to chaiacterize the types and extent
of contamination on and around the site.
The Carolina Transformer site is located in Cumberland County, North Carolina,
approximately one mile northeast of Fayetteville and north of the intersection
of U.S. Highway 301 and River Road.
Carolina Transformer began recycling electrical transformers and capacitors in
1967. In the course of the transformer rebuilding business, Carolina Transformer
handled and stored at the site large numbers of electrical transformers which
contained oil laden with polychlorinated biphenyls (PCB's). In the late 1970's
the North Carolina Department of Natural Resources and Community Development
(NCDNRCD) and EPA collected and analyzed numerous weU-water samples from nearby
homes. The results of the analysis showed no evidence of PCB's but did uncover
evidence of chlorobenzene and other chemical compounds in several of the wells.
In addition, numerous soil/sediment and surface water samples were collected from
suspected contaminated areas on site.
PCB's.
These samples showed the presence of
Phases 1, 2 and 3 were completed and a report was issued in September 1990.
Phase 4 of the Remedial Investigation included the collection of 50 soil samples
from 24 locations off-site. The sample collection locations were situated
southwest of the site in a low-lying area adjacent to the dirt road which borders
the site and from the drainage ditch which flows from the low-lying area to the
Cape Fear River. Additional samples and a duplicate were collected from the pond
area adjacent to the drainage ditch. The samples were analyzed for PCB's. PCB-
1260 was the only contaminant detected in any of the samples. Sediment and
surface water samples were to be collected from the pond; however, no surface
water was encountered in the pond area or the drainage ditch.
ES-1
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The low-lying area southwest of the site was divided into eleven, 100 feet by
100 feet grid areas. The samples collected from locations 2, 3 and 4, which are
adjacent to the dirt road, were the most highly contaminated samples collected
.from the low-lying area. The concentration in the Oto 2 inch BLS samples ranged
between 57,000 ug/kg and 280,000 ug/kg of PCB-1260. The 8 inch to 10 inch BLS
samples contained between 8,600 ug/kg and 79,000 ug/kg of PCB-1260. The .samples
collected from the other 8 grids contained significantly lower concentrations
of PCB-1260.
Twenty soil samples were collected from ten locations in the drainage ditch
which flows to the Cape Fear River. The ten samples collected from Oto 2 inches
BLS all contained detectable concentrations of PCB-1260. The concentrations
ranged from a low of 14,000 ug/kg to a high of 550,000 ug/kg. The ten samples
collected from 8 inches to 10 inches BLS all contained detectable concentrations
of PCB-1260. The concentrations ranged from a low of llOJ ug/kg to a high of
57,000 ug/kg.
Five of the six samples collected from the pond. area contained detectable
concentrations of PCB-1260. All three Oto 2 inch BLS samples contained PCB-
1260 and ranged in concentration from 7,500 ug/kg to 54,000 ug/kg. The
concentration of PCB-1260 in the 8 inch to 10 inch BLS samples ranged between
not detected and 1,800 ug/kg.
ES-2
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REMEDIAL INVESTIGATION REPORT
PMSE 4
OFF-SITE SOIL SAMPLING
CAROLINA TRANSFORMER SITE
FAYETTEVILLE, NORTH CAROLINA
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TABLE OF CONTENTS
SECTION
PAGE
1. 0 INTRODUCTION. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
2.0
3.0
1. 1
1. 2
Site Location .......................................... :. 1 Site History ............................................. 4
SAMPLING STRATEGY. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
SITE DESCRIPTION ............................................... 6
3.1
3.2
3.3
3.4
Land Uses ................................................ 6 Topography and Surface Drainage .......................... 6 Geology .................................................. 6 Hydro geology ....................................... , . . . . . 8
4. 0 SAMPLING INVESTIGATION. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
4.1 Off-Site Soil ..................... : .................... 11
4 .1.1
4 .1. 2
Scope and Methodology ........................... 11 Analytical Results. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
5. 0 REFERENCES. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
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I LIST OF FIGURES
I FIGURE
I 1 Site Location Map ................................................ 2
2 Site and Surrounding Area Map .................................. :. 3
I 3 Site Area Drainage Pattern ............................... , ....... 7
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Soil Sampling Location Map with Grid Areas ....................... 12
Drainage Ditch Soil Sampling Locations ........................... 13
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TABLE
1
LIST OF TABLES
Off-site Soil Samples Data Swnmary Table ...................... 15
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1.0 INTRODUCTION
Sufficient data and information must be available to consider and evaluate hazar~ dous waste site remedial alternatives pursuant to Section 104(b) and (e) of the Comprehensive Environmental Response, Compensation and Liability Act (CERCLA). The work effort to gather the necessary data and information is called a remedial investigation.
A Remedial Investigation (RI) was conducted at the Carolina Transformer site in Fayetteville, North Carolina, by the US Environmental Protection Agency (EPA), Region IV, Environmental Services Division, Hazardous Waste Section (HWS).
This phase of the RI was conducted to characterize the extent of PCB' s contamination in t~e surface and subsurface soils and sediment in the drainage area south of the site.
1.1 Site Location and Description
The Carolina Transformer site is located in Cumberland County, North Carolina, approximately one mile northeast of Fayetteville and north of the intersection of U.S. Highway 301 and River Road (Figure 1). The approximate map coordinates are latitude 35" 03' 08" N and longitude 78" 50' 07" W.
The site consists of approximately 4.8 acres of relatively flat terrain and is bounded on the north by a wooded/swamp-like area which is adjacent to an agricul-tural field and numerous homes; on the west by a dirt road which provides access to two homes; on the south by Middle Road, Larry's Sausage Company and Lundy Packing Company; and on the east by an abandoned home site and an agricultural
field (Figure 2).
Located on the site are a foundation and a variety of buildings of varying sizes. These are situated predominantly towards the front and northeast portion of the property. The western portion of the site is relatively open. Much of the area around the foundation and buildings has been paved with concrete.
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Figure 1
Site Location
Fayetteville, NC
_..,__
FlGUl{E 2
Sl TE AND SUl'.ROUNDING AREA MAP
CAROLJ N/1 TIU1NSFOl{ME!{
FAYETTEV] LL!-:, 1w1n11 CAl<OL l UA
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1.2 Site History
Carolina Transformer began recycling electrical transformers and capacitors in
1967. In the course of the transformer rebuilding business, Carolina Transformer
handled and stored at the site large numbers of electrical transformers which
contained oil laden with polychlorinated biphenyls (PCB's). In the late 1970's
the North Carolina Department of Natural Resources and Community Development
(NCDNRCD) and EPA collected and analyzed numerous well water samples from nearby
homes. No evidence of PCB' s was detected but there was evidence of chlorobenzene
and other chemical compounds in several of the wells. In addition, numerous
soil/sediment and surface water samples were collected from suspected
contaminated areas on site. These samples showed the presence of PCB's.
After the company made no attempts to remove or control the contaminants iden-
tified during the various sampling investigations, EPA, on August 13, 1984 began
an immediate removal action. Clean-up consisted of dewatering the contaminated
swampy area of the site where PCB contaminated surface water pooled and soaked
into the soil. The excavated areas were back fille~ with uncontaminated soil.
Approximately 975 tons of PCB contaminated material was removed from the site
and transported to the Chemical Waste Management disposal facility in Emelle,
Alabama.
The site has been inactive since 1986.
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2.0 SAMPLING STRATEGY
The sampling investigation specified in the August, 1989 Project Operations Plan (POP) was conducted in three phases. Phase 1 of the investigation was conducted in August 1989 and included the collection of surface and subsurface on-site and off.site soil samples, sediment samples, surface water and ground water samples, waste samples and wipe samples. All the samples collected during Phase 1 were analyzed for purgeable organic compounds, acid and base/neutral extractable organic compounds, pesticides, polychlorinated biphenyls (PCB' s) and metals. In addition, selected soil, sediment and waste samples were analyzed for dioxins and furans.
Phase 2 of the investigation was conducted in November 1989 and included the collection of on-site surface and subsurface soil samples. All the samples collected during Phase 2 were analyzed for PCB's. In addition, select samples were analyzed for purgeable organic compounds, acid and base/neutral extractable organic compounds, pesticides, metals and dioxins and furans.
Phase 3 of the investigation, conducted in January 1990, included the installation of five permanent monitor wells. The monitor well samples were analyzed for purgeable organic compounds, acid and base/neutral extractable organic compounds, pesticides, PCB's and metal.s.
A Remedial Investigation report covering phases 1 through 3 was issued in September, 1990. Based on the results from phase 1 of the RI, it was determined that additional. samples would be required from the area southwest of the site and the drainage ditch which flows to the Cape Fear River. Phase 4 of the RI addressed these sampling needs.
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3.0 SITE DESCRIPTION
3. 1 Land Uses
The site is currently not being used for commercial, industrial or recreational
purposes. The 4. 8 acre site is bounded on the north by a wooded/swamp-Like area
which is adjacent to an agricultural field and numerous homes; on the west by
a dirt road which provides access to two homes; on the south by Middle Road,
Larry's Sausage Company and Lundy Packing Company; and on the east by an
abandoned home site and an agricultural field.
The surrounding area includes agricultural, commercial and residential areas.
The main residential areas are located northeast of the site. Agricultural
areas are located north, west and south of the site. Commercial areas are
located to the east and south. A gravel quarrying operation i.s located northwest
of the site.
3.2 Topography and Surface Drainage
The site consists of approximately 4.8 acres of relativ·ely flat terrain. The
area surrounding the site is generally low-lying and swamp-like in character.
The site itself is situated at the headwaters of a drainage ditch or an unnamed
tributary which flows from the west corner of the site less than two miles to
the Cape Fear River. Other drainage ditches flow along Middle Road, west to
the Cape Fear River and east to Locks Creek (see Figure 3).
3.3 Site Geology
The site is located in the Coastal Plain physiographic province of North
Carolina. The mai~ stratigraphic unit at and in the vicinity of the site is
the Tuscaloosa Formation of alluvial origin and Upper Cretaceous in age. The
materials comprising the Tuscaloosa Formation were derived from crystalline
rocks such as granites, gneisses, and schists which compose the adjacent Piedmont
physiographic province. The soils formed from these crystalline materials
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-- - - - - - - - - - - - - - - ----VO Z: 610
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FIGURE 3
SITE DRAINAGE PATTERN
CAROLINA TRANSFORMER
FAYETTEVILLE, NORTH CAROLINA
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APPROXIMATE SCALE
600 0 300 ~----.... I
?H
( IN FEET )
1 inch = 600 ft.
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600
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consist of brown to tan, fine to coarse-grained sands; tan, silty sands; clayey
sands; sandy clays; and grey to blue-grey sandy clays and clays.
The surficial soils at the site consist of the Wickham Series and the Roanoke
Series. Wickham Series soils cover most of the former facility area. These
are well-drained soils that formed in loamy fluvial sediments on terraces of
the Cape Fear River and its major tributaries. The loamy horizon is typically
40 to 60 inches thick and is underlain by sandy alluvial sediments. These are
poorly drained soils that formed in stratified clayey sediments on terraces of
the Cape Fear River and its major tributaries. The loamy and clayey horizons
are generally 40 to 60 inches thick and overlie the stratified sediments
deposited by the river.
3.4 Site Hydrology
The Carolina Transformer Site may be underlain by as many as three ·aquifers.
The alluvial deposits where sand and gravel are present could provide large
yields ·to wells. Available information indicates that the alluvial aquifers
are not presently used for water supply in the area. The sands and clays of the
Cape Fear and Middendorf Formations serve as aquifers in the Fayetteville area.
Wells completed within these formations can be screened over a large interval
which could cover sands and intervening clays. The sands provide much higher
yield and are the most productive aquifers in the region. The bedrock possesses
fracture permeability and is utilized for industrial supplies. A deep bedrock
well was used by Larry's Sausage Company, located adjacent to the site. This
well is 303 feet deep and is completed into the bedrock from 212 feet to the
total depth.
Mr. J. D. Parker, President of the Carolina Sand and Gravel Company, Inc,,
indicated, during a conversation on June 22, 1989, that exploration borings near
the site, to south and northwest, showed a thick clay lens starting at approx-
imately 20 feet below land surface (BLS) and extending down to a least 50 feet
BLS. Copies of the exploration boring logs were later provided to EPA.
The shallow aquifer, located at a depth of five to eight feet below ground
surface, is flowing through a fine to coarse sand layer which varies in thickness
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from six to 13 feet. The shallow ground water appears to flow in a northeasterly
direction. The grey to blue-grey clay located under the upper sand layer is very tough and dry (observed from samples), indicating that the clay is a very good confining layer separating the shallow aquifer from the deeper aquifers.
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4.0 SAMPLING INVESTIGATION
All samples were collected (1) and analyzed (2) in accordance with the Carolina
Transformer. Phase 4. Project Operations Plan. August. 1990. The sampling
investigation was to include the collection of soil, sediment and surface water
samples. However, no surface water was encountered in the pond area or the
drainage ditch. Consequently. the data discussion will refer to all the samples
collected as soil samples.
Samples collected during this phase of the project were designated by the prefix
CT (for Carolina Transformer) followed by a three digit sample number starting
with 801 and continuing consecutively. The next two letters "SL" indicated the
sample matrix as being soil.
A final letter (i.e. ;A or B) was used since multiple soil sam_ples were collected
from the same borehole. The final letter "A" indicated a sample depth of 0
inches to 2 inches and a 11 B11 indicated a sample depth of 8 inches to 10 inches.
For example. the sample number CT-810-SLB will denote the tenth sample collected
is a soil sample collected from 8 inches to 10 inches below land surface (BLS).
Several abbreviations are used in the following sections while discussing the
analytical results. They include:
PCB's
ug/kg
J
polychlorinated biphenyls
micrograms per kilogram
estimated value
N presumptive evidence of material
While discussing the analytical data in the following sections. the prefix "CT"
for each sampling location will be omitted. as will the leading 8 from the three
digit number. For example, sample CT-810-SLB will be referred to as sample 10-
SLB.
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4.1 Soil Sampling
Phase 4 of the investigation, conducted in August 1990, included the collection of 50 soil samples from 24 locations off-site. The sample collection locations were situated southwest of the site in a low-lying area adjacent to the dirt rond which borders the site, and from the drainage ditch which flows from the low-lying area to the Cape Fear River. Additional samples and a duplicate sample were collected from the pond area adjacent to the drainage ditch. The samples were analyzed for PCB's. Sediment and surface water samples were to be collected
from the pond; however, no surface water was encountered in the pond area or the drainage ditch.
4.1.1 Scope and Methodology
The low-lying area southwest of the site was divided into eleven, 100 feet by 100 feet grid areas (Figure 4). The soil samples were collected· from the approximate center area of the grid. Also, four additional aliquots of soil were collected from each grid and composited with the soil sample collected from the center of the area to generate one sample. The four additional sampling locations were located approximately 50 feet from the center of each area at angles of 0°, 90°, 180° and 270° from north. This was performed for each sampling depth. The sampling locations were selected to bracket the drainage ditch and cover the low-lying area adjacent to the site which received runoff directly from the site through a conduit under the dirt road. The drainage ditch in this area is relatively undefined.
Twenty soil samples were collected from ten locations in the drainage ditch which flows to the Cape Fear River (Figure 5). At each locati.on, a sample was collected form Oto 2 inches BLS and from 8 inches to 10 inches BLS. The samples were collected every 100 feet until the dirt road, located to the west of the Larry's Sausage office building, was reached.
Eight samples were collected from 3 locations in the dry pond area. At each location, a sample was collected from Oto 2 inches BLS and from 8 inches to 10 inches BLS. Samples 25-SLA and 25-SLB are duplicates of samples 23-SI.A and
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DR ... lliAIZ DITCH
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160 sc:LE BO 160 --~---·-·-:?
b.;;--:-jEET , I ~ ~ ~----------FIGURE 4
1 inch = 160 ft. SOIL SAMPLING LOCATION
dbEPA MAP WITH GRID AREAS
CAROLINA TRANSFORMER
FAYETTEVILLE, NORTH CAROLINA
-~-----------------
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FIGURE 5
DRAINAGE DITCH SOIL
SAMPLING LOCATIONS
CAROLINA TRANSFORMER
FAYETTEVILLE, NORTH CAROLINA
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APPROXIMATE SCALE
600 O 300 600 ~ ~....J J aw~ ...,
( IN FEET )
1 inch = 600 ft.
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23-SLB, respectively. The analytical results from location 23 will be presented
in the following discussion. The pond appeared to be connected to the ditch near
sampling locations 15 and 20. These areas would allow the pond to receive runoff
from the ditch during periods of heavy rainfall. During a previous
reconnaissance of the area, the pond area was noted to contain water while the
ditch was dry. This suggests that the pond is at a lower elevation than the
ditch. Other than the drainage ditch, no other influent to the pond was
observed, and the area for surface runoff into the pond was minimal.
4.1.2 Analytical Results
All of the samples were analyzed for PCB's. The analytical results for the
individual compounds are provided in data summary Table 1. The laboratory data
sheets are provided in Appendix A. PCB-1260 was the only contaminant detected
in any of the samples.
Twenty-two composite samples were collected from ele_ven locations in and around
the drainage ditch and the low-lying area adjacent to the dirt road which borders
the site. The samples collected from locations 1, 5, 6 and 9 contained no
detectable concentrations of PCB's. Locations 1, 6 and 9 were located in a
farmer's field adjacent to the tree line south-southeast of the drainage ditch.
Location 5 was adjacent to the. dirt road approximately 180 feet west of the
drainage ditch.
The samples collected from locations 2, 3 and 4, which are adjacent to the dirt
road, were the most highly contaminated collected from the low-lying area.
Samples 2-SLA, 3-SLA and 4-SLA contained 200,000 ug/kg, 280,000 ug/kg and 57,000
ug/kg of PCB-1260, respectively. Samples 2-SLB, 3-SLB and 4-SLB contained 79,000
ug/kg, 68,000 ug/kg and 8,600 ug/kg of PCB-1260, respectively.
The concentration of PCB-1260 in the samples collected from locations 7, 8, 10
and 11 was significantly less than the concentration in the samples collected
adjacent to the road. The concentration of PCB-1260 in the O to 2 inch BLS
samples ranged between 400JN ug/kg, in sample 10-SLA, and 4,800 ug/kg, in samples
8-SLA and 11-SLA. The concentration in the 8 inch to 10 inch BLS samples ranged
between 150J ug/kg in sample 10-SLB to 1,100 ug/kg in sample 8-SLB.
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SAMPLE NUMBER
PESTICIDE/PCB COMPOUNDS
PCB-1260 (A.~OCLOR 1260)
SAMPLE NUMBER
PESTICIDE/PCB COMPOUNDS
PCB-1260 (AROCLOR 1260)
SAfl?LE NUMBER
PESTICIDE/PCB COMPOUNDS
PCB-1260 (AROCLOR 1260)
SAMPLE NUt-ffiER
PESTICIDE/PCB COMPOUNDS
PCB-1260 (AROCLOR 1260)
nnnFOOTtlOTES••n*
J ESTIMATED VALUE
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TABLE 1 ANALYTICAL DATA S!JM1ARY CAROLINA TRANSFORMER FAYETTEVILLE, NORTH CAROLINA
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1-SLA 1-SLB Z-SLA 2-SLB 3-SLA 3-SLB 4-SLA 4-SLB 5-SLA 5-SLB 6-SLA 6-SLB 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90_
UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG
200000 79000 280000 68000 57000 8600
7-SLA 7-SLB 8-SLA 8-SLB 9-SLA 9-SLB 10-SLA 10-SLB 11-SLA 11-SLB 12-SLA 12-SLB 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90
UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG VG/KG VG/KG
600J 3SOJN 4800 1100 400JN lSOJ 4800 330 260000 57000
13-SLA 13-SLB 14-SLA 14-SLB 15-SLA 15-SLB 16-SLA 16-SLB 17-SLA 17-SLB 18-SLA 18-SLB 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90
UG/KG UG/KG UG/KG UG/KG VG/KG VG/KG UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG
220000 6000 170000 19000 74000 760 46000 llOJ 94000 22000 100000 8600
--
19-SLA 19-SLB 20-SLA 20-SLB 21-SLA 21-SLB 22-SLA 22-SLB 23-SLA 23-SLB 24-SLA 24-SLB 25-SLA 25-SLB 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90 08/07/90
UG/KG
550000
VG/KG
36000
UG/KG
14000
UG/KG
4700
UG/KG
17000
UG/KG
4300
UG/KG
30000
VG/KG UG/KG
54000
UG/KG
1500
VG/KG
7500
VG/KG
1800
UG/KG
26000
UG/KG
2000
N PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL MATERIAL WAS ANALYZED FOR BUT NOT DETECTED
15
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The ten samples collected from the drainage ditch from O to 2 inches BLS all
contained detectable concentrations of PCB-1260. The concentrations ranged from
a low of 14,000 ug/kg in sample 20-SI.A to a high of 550,000 ug/kg in sample 19-
SI.A. With the exception of samples 17-SI.A, 18-SI.A and 19-SI.A, the concentration
of PCB-1260 tended to decrease as the distance from the site increased. The
ditch in the area of sampling locations 17, 18 and 19 was not as defined as
other sections of the ditch. That is, the ditch was wider and more shallow.
This area was also adjacent to the dry pond.
water and increased sedimentation in the
concentration of PCB-1260.
This may of allowed for standing
area resulting in the higher
The ten samples collected from the drainage ditch from 8 to 10 inches BLS all
contained detectable concentrations of PCB-1260. The concentrat_ions ranged from
a low of llOJ ug/kg in sample 16-SLB to a high of 57,000 ug/kg in sample 12-
SLB. There was no apparent trend between the concentration of PCB-1260 and the
distance from the site. The concentration of PCB-1260 from sampling locations
17, 18 and 19 were generally higher than those from the sampling locations
immediately up and down gradient.
Five of the six samples collected from the pond area contained detectable
concentrations of PCB-1260. All three Oto 2 inch BLS samples contained PCB-
1260 and ranged in concentration from 7,500 ug/kg in sample 24-SI.A to 54,000
ug/kg in sample 23-SI.A. Samples 23-SLB and 24-SLB contained 1,500 ug/kg and
1,800 ug/kg of PCB-1260, respectively.
16
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5.0 REFERENCES
1.
2.
3.
United States Environmental Protection Agency, Region IV, Environmental Services Division, Engineering Support Branch Standard Operating Procedures and Quality Assurance Manual, April 1986.
United States Environmental Protection Agency, Region IV, Environmental Services Division, Analytical Support Branch Operations and Quality Control Manual, June 1985.
United States Environmental Protection Agency, Environmental Monitoring Systems Laboratory, Aerial Photographic Analysis of Carolina Transformer, East Fayetteville. North Carolina, TS-AMD-87712, July 1987.
17
- - ----- - - --SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. - - -- --09/19/90 PESTICIDES/PCB'S DATA REPORT .. .. .. ..
PROJECT NO. 90-785 SAMPLE NO. 48891 SOURCE: CAROLINA TRANSFOP.MER STATION ID: 1-SLA
UG/r,G ANALYTICAL RESULTS
tJA ALDRIN NA HEPTACHLOR NA HEPTACHLOR EPOXIDE NA ALPHA-BHC NA BETA-BHC NA GAMMA-BHC (LINDANE) NA DELTA-BHC NA ENDOSULFAN I ( ALPHA)
NA DIELDRitJ NA 4,4·-DOT tP,P'-00Tl tJA 4,4'-DDE (P,P'-DDE) NA 4,4'-DDD (P,P'-DDD) NA ENDRIN tJA ENDOSULFAN II CBETAJ NA ENDOSULFAN SULFATE
tJA CHLORDANE (TECH. MIXTURE l /1 210U PCB-1242 (AROCLOR 1242)
210U PCB-1254 (AROCLOR 1254) 210U PCB-1221 CAROCLOR 1221)
SAMPLE TYPE: SOIL BY: D THOMAN ST: NC PROG ELEM: SSF COLLECTED CITY: FAYETTEVIL COLLECTION START: 08/07/90 1025 STOP: 00/00/00
UG/t<.G ANALYTICAL RESULTS
210U PCB-1232 (AROCLOR 1232) 210U PCB-1248 CAROCLOR 1248)
210U PCB-1260 CAROCLOR 1260) 210U PCB-1016 (AROCLOR 1016) NA TOXAPHENE NA CHLORDENE /2 NA ALPHA-CHLORDENE /2 NA BETA CHLOROENE /2 NA GAMMA-CHLORDENE /2 NA t-HYDROXYCHLORDfNf /2 NA GAMMA-CHLOROAf~E /2 NA TRANS-NONACHLOR /2 NA ALPHA-CHLOROANI' /2 NA CIS-NONACHLOR /2 NA OXYCHLORDANE l OCTACHLOREPOX IDE) /2 tJA METHOXYCHLOR NA FNOR!N KETONE 12 PERCENT MOISTURE
.. .. ..
••
• • • FOOHJOTES• • • •A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVErJ •U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITAT!ON LIMIT. C-CONFIRMED BY GC/MS 1. WHEN NO VALUE IS REPORTED. SEE CHLORDMJE CONSTITUENTS. 2. COtJSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-
--- - --- -
PtSIJCJDtS/PCB'S DATA REPORT -- - - -
SAMPLE AND ANALYSIS MANAGEMENT W5TEM
EP.l~--P.EGIOM !V ESD. AT:--lENS, CA.
••••• .......... ,i: ................ ,..,.t*'fTT-l':tS
PROJECT NO. 90-785 SAMPLE NO. 48892 SAMPLE TYPE: SUJL ' . .
SOUR\,f: CAROLIN/\ TRANSFORMER
- - -
BY: D THOMAN ST: NC
--..
•• .. .. STATION ID: 1-SLB
PROG ELEM: SSF COLLECTED CITY: FAYETTEVIL COLLECTION START: OG/07/90 1035 $TOP: 00/00/00
L!C/KG ANAL YT I CAL RESULTS
N,~ ALDRif.J 520U PCB-1232 (MWCLOR i232) NA. ~tPIACHLOR 520ll P'-'B-12~8 l f.~OCLOR 1243) !✓A HH·TACHLOR EPOXJDE 520U PCB-1260 ( ARQ(,IOR 1?ROl M.'\ /\:. .. Yi-!A-C: !C ~20U PCB-1016 (AROCLOR 1016) NA BtfA-BHC NA TOXAPHENE IJA GAMMA-BHC ( LINDANE) NA CHLORDENE /2 ~IA DEL T.ti.-8HC NA ALPHA-CHLOKDENE /2 NA ENDOSULFAN T (ALPHA_) .. ~ OCTA 1...,nLu"ur: Ne /2 ~~:'\ DIE!..DRIN N.lli. GAMMA-C!--!L.OROE~JE /2 NA 4,4'-lllJ1 I_P,P'-QQTJ NA i -HY(H<UX Vl .. Hlll~LJl:N!:: /2 tJA 4_4'-DDE (P.P"-DDEi N,\ GAMMA-CHLORD/11~[ /2 NA 4,4"-DDD (P. P' ··ODO) NA I J.l Af\1:--!'-Jl~IN_ti_f_"H!..OR 10 i-iM [i-iDR I hi NA ALPHA-CHLOR~ANf' /2 ~lA ENCOSULF Ai-J l I (SETA) NA CIS-NONIICHLOR /2 NA rnon5ULF~N SULt-,:/1,TE ;-JA OXYCHI_OF<UAfl.!!: (Of,lACYLOREPOXIDEJ /2 ~JA CHLORDANE (TECH. i>HXTUREl /1 NA METHOXYCl !LOR 5:.,,()lJ Prn-1242 ( t,ROCLOR 1242) NA f.Nflf< IN KI: fONE 520U PCB-1?54 ( AROCL0R 12S4l 7.6 PERCENT MOISTURE 520U PCB-1.221 (AROCLOR ~ 221)
•••FOOTNOTES•••
-
0\1/22/90 . ' . ... .. ..
• • ••
TA-AVE~AGE VALUE •WA-NOT ANALY7FO •NAI-JMIERfERENCES •J-ESTIMATED VALUE •N-PRESUM?TIVE EVIDENCE OF PRESENCE Uf M~TERIAL
•K-ACTUAL VALUE IS r,NOWtJ TO BE LESS THAtJ VALUE GIVEN •L-ACTUAL VALLIE IS KNOWN TO BE GREATER THAN VALUE GIVEtJ
•U-MATERIAL WAS ANALYZff) FOR tlUT ,-mr DETECTED. T~E NUMSER rs TIIE r.~HJir.~:JM OUANTIT.4TION LiMIT. C-(OMFIRMED BY GC/MS
1. WHE~l t!O 'JALUE IS REPORT[D. SEE CHLORDANE CONSTITUFNTS. 2. CO,..lST!TIJnJTS OR ,•.~ETABOLITES OF TECHIJICAL CHLORDANE.
-
-·-·---
PESTICIDES/PCB'S DATA REPORT
" ..
" • •
PROJECT IJO. 90-785 SAMPLE SOURCE: CAROL INA TRANSFORMER STATION ID: 2-SLA
- - -- - --- --- -
IJO. 48923
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHErJS, GA.
SAMPLE TYPE: SOIL PROG ELEM: SSF COLLECTED CITY: FAYETTEVIL COLLECTION START: 08/07/90
BY: D THOMAN ST: NC 1540 STOP: 00/00/00
-09/19/90
•• •• .. .. ♦T4 ♦ ♦ ♦ ♦ ♦ t * * * * * * * * * * * * * * * *TT T * T TT T T *TT T * * T T TT T TT $TT TT T T T T TT TT T TT TT TTT UG/r,G AIJALYTICAL RESULTS IJG/KG ANALYTICAL RESULTS
NA ALDRIN 4900U PCB-1232 ( AROCLOR 1232) NA HEPfACHLOR 4900U PCB-1248 (AROCLOR 1248) NA HEPTACHLOR EPOX IDE 200000 PCB-1260 (AROCLOR 1260) NII ALPIIII-BIIC 4900U PCB-1016 (AROCLOR 1016) NA BETA-BHC NA TOXAPHENE NA GAMMA-BHC (LINDANE) NA CHLOROENE /2 NA DELTA-BHC NA ALPHA-CHLOROENE /2 NA rnoOSULFAN I (ALPHA) NA BETA CHLOROENE /2 NA DIELDRIN NA GAMMA-CHLORDENE /2 NA 4,4'-0Df (P.P'-ODTJ NA 1-HYOROXYCHLOROENE /2 IJA 4.4'-00E (P.P'-DDE) NA GAMMA--CI ILORDAIJE /2 NA 4.4'-DDD (P,P'-DDO) NA TRANS-NONACHLOR /2 NA [NORIN NA ALPHA-CHLOROANE /2 IJA EIJDOSULFAN II (BETA) NA CIS-NONACHLOR /2 NA ENOOSUL•AN SULFATE NA OXYCHLOROANE (OCTACHLOREPOXIOE) /2 NA CHLORDANE (TECH. MIXTURE) /1 NA METHOXYCHLOR 4900U PCB-1242 (AROCLOR 1242) NA ENOR!N KETONE 150000U PCB-1254 (AROCLOR 1254) 14 PERCENT MOISTURE 4900U PCB-1221 ( AROCLOR 1221)
•*•REMARKS•••
•*•FOOTNOTES•••
•A-AVERAGE VALUE •IJA-NOT ANALYZED •NAI-!NTERFERENCES •J-EST!MATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATER!AL •r.-ACTUAL VALUE IS r,NOWIJ TO BE LESS THAIJ VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN •LI-MATERIAL WAS ANALYZED FUR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. C-CONFIRMEO BY GC/MS 1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS 2. CONSTITUENTS OR METABOLITES Of TECHNICAL CHLORDANE.
-
-· --- -- -
PESr1c10ES/PCB'S DATA REPORT
··••*•"•"*********"'*
- -- - -
SAMPLE AtJO ANAL VS IS MANAGEMENT SY5 TEM
EP.ti.-REG!ON !V ESD, ATHENS, GA.
-- -- -
* * • * T ~ T :f. • • • ... ~ ............... -............ . ...
•• .. PROJECT NO. 90-785 SAMPLE NO. 489,4
SOUR ff: CAROL Ir-!/\. TR.ti.MSFORM=P. SAMPLE TYPE: SOIL PROG ELEM: SSF COLLECTED BY : D THOMAIJ
ST: NC
" .. STATION ID: 2-SLB
;JA ALDRIN
r-!A HtP I /l.CHLOR
l~A HEr~TACHLOR EPOX !DE
~J!\ At...r: 1,,-, -e: ic NA BtlA-BHC NA GAMMA-BHC C LI NDANE l
MA DEL T.t..-BHC
!<A ENDOSULF AN I ( ALPHA)
t~A D!ELCRIIJ NA d . 4' -Pl)l 1_ o. P, -o~n ,
tJA 4.4'-DDE (P.P'-ODE)
MA 4.4'-00D (P. P' ··-DDD)
i'4A LNDRiN tJA E:JCOSULF AfJ II (SETA l NA FNOQSIJLFA.M SULf .'\ fE
~JA CHLORUKf'>iE (TECH. Mi XTURE)
9(Jl)l)U PCB-1242 (/\ROCLOR 1242) 750000 PCB-1254 ( AROCLOR 1 ?54.,
90000 PCB-1221 ( AROCLOR 1221 l
• • • FOOHJOTES• ••
./ 1
CITY: ~AtETTEVIL
COL.L.ECTimJ START: 08/07/90 1600
IJG/!'.G
DOCCU PCB-1232 (AROCLOR 1232)
9000U PCtl-12118 (AROCLOR 1248) 79000 PCB-1260 IAROCLOR 1?60)
90000 PCB-1016 ( AROCLOR 1016) NA TOXAPHENE NA CHLORDENE /2 NA ALPHA-CHLURDENE /2 IJA BETA CHLORDFNf /2 NA GAMMA-CHLORDENE /2 NA l-HYt)R:0X:Y01LORDt=Nf. /2 t;A GAM~A-CHLO~UANE /2 NA r ~Al\l':,-MOM.o.•.:HLQR M
NA ALPHA-CHLORflANF /2 NA CIS-NONACHLOR /2
5TOP: 00/00/00
NA (JXYCH!. t)RL)ANI: (OCTACHLOP.EPOXIDE) /2 ~~A METHOXYCI !LOR NA fNllR!N KETONE
8.8 PERCENT MOISTURE
-U\J/22/90
tA-AVEr-:AG[ VALUE •l..iA-NGT ANALV7F.0 •~Al-!NIERfERENCES ""'J-ESTH,~ATED VALUE :rN-~R[SUM;::TIVE CVIDEt-KE OF PRESENCE Uf MATERIAL •r,-ACTU.•L v.~LUE IS Y-tJOWt) TC BE LE3S THAN VALUE GIVEN •L-ACTUAL VALLIE 15 KNOWN TO B~ GREATER THAN VALUE GIVW •U-MATERIAL WAS ANAI.Y7ffl FVH ~lll NOT DETECTED. THE NUMBER IS Tl:E MINIMUM QUANTITATION LIMIT. C-CONFIRMED BY GC/MS
1. WHHJ NO VALUE IS REPORT[D. SEE CHLORDANE CONSTiTtJFNTS. 2. CONSTITUENTS OR METABOLITES OF TECHIJICAL CHLORDANE.
-
- - - -- -- - - - - -- -
SAMPLE Al,D ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD. ATHENS, GA. PEST!CIDES/PCB'S DATA REPORT ... .. .. .. ..
• * • * • * * * • * • • • • • * * • * * • * • * • * • • * * PROJECT NO. 90-785 SAMPLE NO. 48925 SAMPLE TYPE: SOIL SOURCE: CAROL I fJA TRANSFORMER STATION ID: 3-SLA
UG/KG ANALYTICAL RESULTS
NA ALDR I IJ NA HEPTACHLOR NA HEPTACHLOR EPOXIDE IJA ALPHA-BHC NA BETA-BHC NA GAMMA-BHC (LINDANE) NA DELTA-BHC NA ENDOSULFAN I ( ALPHA) NA DIELDRIN NA 4 4'-001 (D.P'-DDT) tJA 4:4'-DDE (P.P'-ODEl NA 4.4'-0DD (P,P'-DDD) NA ENDRJN IJA ENDCSULF AfJ II (BETA l NA fNDQSULFA.N SULFATE tJA CHLORDANE { TECH. MIXTURE) /1 3600U PCB-1242 (AROCLOR 1242)
2SOOOOU PCB-1254 (AROCLOR 1254) 3600U PCB-1221 ( .4ROCLOR 1221 )
•••FOOTNOTES•••
• • • * * * • • • • * • * • • • • * • * • • * • • • * * • PROG ELEM: SSF COLLECTED BY: D THOMAN ST: NC CITY: fAYETTEVIL COLLECTION START: 08/07/90 1610 STOP: 00/00/00
UG/KG ANALYTICAL RESULTS
3600U PCB-1232 (AROCLOR 1232) 3600U PCB-1248 (AROCLOR 1248)
280000 PCB-1260 ( AROCLOR 1260)
3600U PCB-1016 (AROCLOR 1016) NA TOXAPHENE NA CHLORDENE /2 NA ALPHA-CHLORDENE /2 NA BETA CHLORDENE /2 NA GAMMA-CHLORDENE /2
t,iA 1-HYORUXYCHLORDENE /2
~~A GAMMA-CHLORDANE /2 NA TRANS-NONACHLOR /2 NA ALPHA-CHLORDANE /2 NA CIS-NONACHLOR /2 NA OX ¥CHLORDANE (OCTACHLOREPOXIDE) /2 NA METHOXYCHLOR NA fNORIN KETONE 13 PERCENT MOISTURE
-09/19/90
• • • ... .. ..
•• ••
•A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-ESTJMATED VALUE •ti-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE JS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEtJ •U-MATERIAL WAS ANALYZED FOK ~Ul NOT DElECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMil. C-CONFIRMED BY GC/MS 1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSl!TUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-
--·---PEST!CIDES/PCB'S DATA REPORT ... ,. .. .. ..
··••"-••--**• .. ••• PROJECT NO. 90-785 SAMPLE SOURCE: CAROL I NA TRANSFORMER STATION ID: 3-SLB
-------·-----SAMPLE AIJD ANAL VS IS MANAGEMENT SYSTEM EPA-REGION JV ESD, ATHENS, GA.
• • • • • • • • • * • * * • • • • • NO. 48926 SAMPLE TYPE: SOIL • • • • • • • • • • • • • • • • • • • • • • • • • PROG ELEM: SSF CITY: FAYETTEV!L COLLECTION START:
COLLECTED BY: D THOMAN ST: NC 08/07/90 1625 5 TOP: 00/00/00
-
09/19/90 ... .. ..
•• . . ••• • • • ♦ ••••••• * • *. * •••••••• t * * • * •• ~ ••• * ••••••••••••••• * * ••• * •••••••• UG/r,G ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS NA ALDRIN 3700U PCB-1232 (AROCLOR 1232) NA HEPTACHLOR 3700U PCB-1248 (AROCLOR 1248) NA HEPTACHLOR EPOX!DE 68000 PCB-1260 (AROCLOR 1260) NA ALPHA-BHC 3700U PCB-1016 (AROCLOR 1016 J NA BETA-BHC NA TOXAPHENE NA GAMMA-BHC (LINDANEJ NA CHLORDENE /2 NA DELTA-BHC NA ALPHA-CHLORDENE /2 IJA ENDOSULFAN I (ALPHA) NA BETA CHLORDENE /2 NA DJELDRIN NA GAMMA-CHLORDENE /2 NA 4.4"-0DT t•.P'-DDTJ NA 1-HYOROX YCHLORDfNf /2 NA 4,4'-DDE (P,P'-DDEl NA GAMMA--CI H .. ORDAf~[ /2 NA 4,4'-00D (P,P'-000) NA TRANS-NONACHLOR /2 NA [NORIN NA ALPHA-CHLOROANF /2 NA EtJDOSULF AtJ I I (BETA) NA CJS-NONACHLOR /2 NA ENDOSULFAN SULFATE NA OXYCHLOROANE (OCTACHLOREPOXIDE) /2 NA CHLORDANE (TECH. MIXTURE) /1 NA METHOXYCHLOR 3700U PCB-1242 (AROCLOR 1242) NA fNDR!N Kl:TONE 65000U PCB-1254 (AROCLOR 1254) 12 PERCENT MOISTURE 3700U PCB-1221 ( AROCLOR 1221)
•••FOOTNOTES•*• •A-AVERAG[ VALUE •IJA-NOT ANALYZED •NAJ-INTERFERENCES •J-EST!MATED VALUE •N-PRESUMPTJVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE JS KNOWN TO BE GREATER THAN VALUE GIVEN •U-MAT[RJAL WAS ANALYZED Fllk BUT NOT DETECTED. THE NUMBER IS THE MWIMUM QUANTJTATIDN LIMIT. C-CONFIRMED BY GC/MS 1. WHEN tJO VALUE JS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-
-·-- - - - -
PESfJLIDES/PCB'S DATA REPORT
--- - -
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EP.A.-P.EGIO!-l I'.' ESD, ATHEt~S. CA. - - - --
" •• PROJECT NO. 90· 735 SAMPLE
SOURCF: CAROL INA TP.A"JSFOP..MER STATIOJJ ID: 4-SLA
NO. 48927 SAMPLE TYPE: SOIL PROG ELEM: SSF COLLECTED
CITY: fAYETTEVIL COLLECTION START: 08/07/90
BY: D THOMAN
ST: NC •• • •
uc;r.c
r~ . .l. NA
1-.iA
t!:'\ NA NA "A NA
~J/\ NA
tJA NA
;J:,.
~JA NA
tJA
61i(JU
55000U 660.U
A~ALYTiCAL RESULTS
ALDRHJ HE.PTACHLOR
HEPTACHLOR EPuX IDE
,. ' <'JI.I~ "'-' "'' Bl:C RflA-BHC GAMMA-□HC ( L!NDANE)
DEL T,6.-8HC ENDOSULFAN l ( ALPHA)
QIELDRitJ
4, 4' -f)[)'! ry. P'-DDT)
4,4'-DDE (P,P"-DDEl
4,4'-DDD (P,P' DOD)
i:i-.iU~ ii-J WDOSULF AIJ :i (BETA)
Ft,J[)OC..IJl__.f ft.M SIJLF/\TE
CHLORDMi-.iE \ TECH. MIXTURE) /I PCB-1242 { 1\ROCL'.JR 1242) PCB-1254 ( AROCLl1R 125'-I)
PCB-1221 {AROCLOR 122i)
...... fOOTNOTfS•••
1520 STOP: 00/00/00
I_Uj/!(G ANALYTICAL R[SULTS
060U PCB ·i232 \AROCLOR i232)
660ll P<.:!:~-12'18 ( AP.OCLCP. 1243) 57000 PCB-1260 ( AROCLOR 1?0())
660U PCB-1016 (AROCLOR 1016)
NA TOXAPHENf
NA CHLORDENE /2 NA ALPHA-CHLORDENE /2
iJA BETA CHLORDi:Nf. /2
!-J/l., GAMMA-CHLORDENE /2
hiA i -H·vot<(IK VCHLORUtNf /2
n!I. GA~,lMA--<:HLCRO,\i.,j[ /2
NA I l-({J.f'l.I$-Ml_lM.tJ..1:~!..0R I?
NA ALPHA-CHLOROANF ~12 NA C JS-NotJP,CHLOR /2
NA OX Vt".Hl .. (lf<l)Ar-.lE (OrTArHLOREPOXID!c) /2
N:'\ ~.~ETHCXYCHLOR NA FNllR]N ~.E'IONE
12 PERCEJJT MOISTURE
-0~/22/90
•• •• •• ..
TA· AVE~AGE v:..LUE .. j,,jA-NOT Ai,JAL'v"/.FIJ •I\IAl-!MIERFERENCES ~J-ESTIMATED VALUE i:J-PR[SUMPTIVE EVIDENCE OF PRESENCI: or MA.TERIAL •Y.-ACTUAL VALUE IS KIJQ\•IIJ TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS rnOWN TO BE GREATER THAN VALUE GIVEIJ
4LJ-MATERIAL WAS ANALY7.FO F1Jfs? t\lJT !'!OT DE-TECTED. THE ~!U~mER IS THE MI:,iIM:JM Qi.JAfHITATION LIMIT. C-COMFIRMED BY GC/MS
1. WHE~! NO 1v',~LUE IS RE::'ORT[D. SEE CHLORDANE CONSTITUFNTS 2. 1:0MSTIT!JENTS O?. METABOLITES Of TECHf..JICAL CHLORDANE.
-
-·-· ---- -- - - - - - -- - - -
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.
••• * * * • * ••••• * • * * *. * ••• * * • * * * * * * * • • • " PROJECT NO. 90-785 SAMPLE NO. 48928 SAMPLE TYPE: SOIL •• SOURCE: CAROLINA TRANSFORMER •• STATION ID: 4-SLB • •
PROG ELEM: SSF CITY: FAYETTEVIL COLLECTION START:
COLLECTED BY: 0 THOMAN ST: NC 08/07/90 1535 STOP: 00/00/00
09/19/90 . ' . ...
•• •• •• ••
+♦♦ + ♦ + ♦ ♦ ♦ ••• * •• *. * * * *. * * •• * * * * * * * • * * * * • * • ' •• *. * * •• * * * * •••••••••• ' ••• UG/r,G ANALYTICAL RE SUL TS UG/KG ANALYTICAL RE SUL TS
NA ALDRW 1500U PCB-1232 ( AROCLOR 1232) NA HEPTACHLOR 1500U PCB-1248 (AROCLOR 1248)
NA HEPTACHLOR EPOX!DE 8600 PCB-1260 (AROCLOR 1260)
NA ALPHA-BHC 1 SOOU PCB-1016 (AROCLOR 1016) NA BETA-BHC NA TOXAPHENE NA GAMMA-BHC (LINDANEJ NA CHLORDENE /2
NA DELTA-BHC NA ALPHA-CHLORDENE /2 IJA ENDOSULFAN I (ALPHA) NA BET A CHLORDENE /2 fJA DIELORHJ NA GAMMA-CHLOROENE /2 NA 4,4'-DDT CP.P'-DOT) NA 1-HYOROXYCHLORDENE /2 NA 4,4'-DDE CP.P'-DDE) NA GAMMA ·CHLORDAIJE /2 NA 4,4'-DDD CP,P'-DDDJ NA TRANS-NONACHLOR /2 NA ENDR IN NA ALPHA-CHLORllANE /2 fJA ENDOSULFAN II C BET A) NA CIS-NONACHLOR /2 NA ENDOSULFAN SULFATE NA OXYCHLORDANE (OCTACHLOREPOXIDE) /2
NA CHLORDAIJE C TECH. MIXTURE) /1 NA METHOXYCHLOR 1 soou PCB-1242 (AROCLOR 1242) NA F NllR IN KETONE
8500U PCB-1254 (AROCLOR 1254) 9 PERCENT MOISTURE
1500U PCB-1221 C AROCLOR 1221)
***REMARKS••*
•••FOOTNOTES*** •A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-JNTERFERENCES •J-ESTIMATEO VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GTVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN •LI-MATERIAL WAS ANALYZED FIJR ~I.IT flOT DETECTED. THE NUMBER IS THE MINIMUM OUANT!TAT!ON LIMIT. C-CONFIRMEO BY GC/MS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-
-·-· ------ - - - - - -- - --
PESTICIDES/PCB'S DATA REPORT ... .. .. .. ..
• ' • • • • * • • • * • • • • • • • • •
PROJECT NO. 90-785 SAMPLE NO. 48921 SOURCE: CAROL I flft. TRANSFORMER STATION JD: 5-SLA
UG/KG AIJALYT!CAL RESULTS
NA ALDRIIJ NA HEPTACHLOR NA HEPTACHLOR EPOX IDE NA ALPHA-BHC
NA BETA-BHC
NA GAMMA-BHC (LJNDANE) NA DELTA-BHC NA ENDOSULFAN I (ALPHA) NA DJELDRIN NA 4,4'-DDT (P.P'-DDTl NA 4,4'-DDE (P.P'-DDE) NA 4,4'-DDD (P,P'-DDD) NA ENDRIN NA EIJDOSULFAIJ II (BETA) NA ENOOSIJLFAM SULFATE NA CHLORDAl,E (TECH. MIXTURE) /1 21nu PCB-1242 (AROCLOR 1242) 210U PCB-1254 (AROCLOR 1254) 210U PCB-1221 ( AROCLOR 1221 )
•••FOOTNOTES••*
SAMPLE AIJD ANALYSIS MANAGEMENT SYSTEM EPA-REGION JV ESD, ATHENS, GA.
• • • • • * • .. " * • • • SAMPLE TYPE: SOIL BY: D THOMAN ST: NC
PROG ELEM: SSF COLLECTED CITY: FAYETTEVIL COLLECTION START: 08/07/90 1630 STOP: 00/00/00
UG/KG ANALYTICAL RESULTS
210U PCB-1232 (AROCLOR 1232) 210U PCB-1248 (AROCLOR 1248) 210U PCB-1260 ( AROCLOR 1260) 210U PCB-1016 (AROCLOR 1016) NA TOXAPHENE NA CHLORDENE /2 NA ALPHA-CHLORDENE /2 NA BETA CHLORDENE /2 NA GAMMA-CHLORDENE /2 NA 1-Hl'OF<l)X VCHLORDENE /2 tJA GAMMA·-CI lLORDHN[ /2 NA TRANS-NONACHLOR 12 NA ALPHA-CHLOROANF /2 NA CIS-NONACHLOR /2 NA OXYCHLORDANE (OCTACHLOREPOXIDE) /2 NA METHOXYCHLOR NA fNORIN KETONE 11 PERCENT MOISTURE
•••REMARKS"•*
09/19/90
• • • ... .. •• •• ••
•A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-ESTJMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •Y.-ACTUAL VALUE JS KNOWN .TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE JS KNOWN TO BE GREATER THAN VALUE GIVEIJ
•U-MATERIAL WAS ANALYZED FUR euT NOT DETECTED. THE NUMBER IS THE MINIMUM OUANT!TATJON LIMIT. C-CONFJRMED BY GC/MS 1. WHEN NO VALUE JS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-
- - -- - ---- - -- -- - --
Pb r l C llJt 5/PCB' S DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SVS TtM
EP.ti.-P.EG!Ot-1 IV ESD. ATHEtJS, GA. ... ♦ ♦ ♦ ♦ • "-" • "•"'• * ** *••••• '"'•••'tT -r:tt: PROJECT NO. 90 -785 SAMPLE NO. 48922 SAMPLE TYPE: 501 L • • • .. • ♦ • ♦ • • .. • • • .. • • • .. • * • • • • .. • .. ..
SOURCE: C A.ROL I NA TRANSFOR,IER STATION ID: 5-SLB
UC,'Y-G
/~A
• • * • * * • * • • • * • .. • T T T T ~ .. .. T .. ~ Af~/,L'r'TICAL RESULTS
MA
hiA
~J,'\ NA NA MA
NA
~Jt\ NA
NA NA ;-,;;.,
~JA NA
tJA s~ou 520U
520U
ALDr\IN HEP I A.CHLOR
Hi:Vi ACHLOF< EPUX JUE /',:_f'tl,'\ -et :c
Rel A-BHC GAMMA-BHC ( LINDANE l
DEL T t>.-BHC ENDOSULFAN
~I~Lr:RUJ l ( ALPHA)
4 ,4'-l)!Jf (P.P'-DDTJ ~.4'-DDE (P.P'-DDEl 4,4'-DDD
Li-iURiN
( P ,I='" ·-DDD)
ENDOSULF A1.J J; {SETA) FJ\IOOSI.ILF~.~J SULf-".",fE CHLGRDAi-JE (TECH. MIXTURE)
PC9-1242 (IIROCLOR 1242) PCB-1254 (AROCI_OR 1 :,54 J PCB-1221 ( AROCLOR 1221)
•••FOOTNOTE:=.,,,
/1
PROG ELEM: SSF CITY: fAYETTEVIL COLLECTION START;
COLLECTED BY: D THOMAN ST: NC 08/07/90 1650 STOP: 00/00/00
♦ • ♦ • .. • • • • .. • .. • • • .. • * * * *
Jl~t~r \ITTl""'~I ...... ,.., .. "T"r ,..,.,~,....~ 1 I J.\.,ML. I\L-•UL I~ 1.1r.:vr.G
s~ou PCS-1232 ( AROCLOR 1232) 5201,1 PCB-1248 { /\ROCLOR 1248) 520U PCB-1260 ( AROCLOR 1260) 520U PCB-1016 NA TOXAPHENE ( AROCLOR 1016)
NA CHLORDENE /2 NA ALPHA-CHLORDENE /2 t..:A BETA CHLORDfNE /2 N.ti. GAMMA-CHLOROENE /2 NA 1-H'v(1t<UXYCHLOKDFNF. /2 ~~,. GA~l,~.lA-CHLORD/\i.JE /2 NA l ~A/'1.1~-M•.lM,o..,;H!...OR ,,,
NA ALPHA-CHLORDANF /2 NA CIS-NON/\CHLOR /2 NA OX v·CHI.OF<UANI: (OCTAC,~LOREPOXIDE) /2 NA METHOXYCI ILOR NA FNDR!N KETONE 6.3 PER.CEi,JT MOISTURE
ll\l/22/9D
' ' ' "' •• •• ••
TA·-AVE~:..GE VALUE •i-JA-hiOi ANAL'v"7FD •MAl-IMIERFERHJCES *J-ESTIMATED VALUE •:J-PR[SUMPTIVE EVIDENCE OF PRESENCt Of MATERIAL •K-ACTLIAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUA! VALUE IS ~.NOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANAL V2FI) Fuw ~I.IT !'>JOT DETECTED. THE W.!MBER IS TIIE MHJIMUM OUAI-JTITATION LIMIT. C-CO~JFIRMEO BY GC/MS
1. \'JHHJ NO VALUE IS REPGRT[U. SEE CHLORDANE CONSTITUFNT':, 2. CO~JST!TL'E~!TS OR ~.~ETABOLITES OF TECHNICAL CHLORDANE_
-
----- - - -- - - --SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD. ATHENS. GA. - -- ---
PESTICIDES/PCB'S DATA REPORT 09/19/90 ... .. .. .. ..
····•-·*•*••······"···"·"""*"" PROJECT NO. 90-785 SAMPLE NO. 48899 SAMPLE TYPE: SOIL SOURCE: CAROLINA TRANSFORMER STATION ID: 6-SLA
UG/KG ANALYTICAL RESULTS
IJA ALDRIN NA HEPTACHLOR 1,A HEPTACHLOR EPOXIDE NA ALPHA-BHC NA BETA-BHC NA GAMMA-BHC (LINDANEl NA DELTA-BHC l,A ENDOSULFAN I ( ALPHA) NA DI ELDR IIJ NA 4.4'-0DT (D.P'-DDT)
NA 4.4'-DDE (P.P'-DDE) NA 4.4'-DDD (P.P'-DDD) NA [NORIN
~JA EIJDOSULF AIJ I I t BET A) NA ENDOSULFAN SULFATE NA CHLORDANE (TECH. MIXTURE) /1 300U PCB-1242 (AROCLOR 1242) 300U PCB-1254 (AROCLOR 1254) 300U PCB-1221 ( AROCLOR 1221 )
• • • BY: D THOMAN ST: NC PROG ELEM: SSF COLLECTED CITY: FAYETTEVIL COLLECTION START: 08/07/90 1120 STOP: 00/00/00
UG/KG ANALYTICAL RESULTS
300U PCB-1232 ( AROCLOR 1232 l 300U PCB-1248 CAROCLOR 1248) 300U PCB-1260 ( AROCLOR 1260) 300U PCB-1016 (AROCLOR 1016) NA TOXAPHENE
NA CHLORDENE /2 NA ALPHA-CHLORDENE /2 NA BETA CHLORDENE /2 NA GAMMA-CHLORDENE /2 NA 1-HYDR.OXYCHLORDfNE /2 NA GAMMA-CHLORiJAi~[ /2 NA TRANS-NONACHLOR /2 NA ALPHA-CHLOROANF /2 NA CIS-NONACHLOR /2 NA OXYCHLORDANE tOCTACHLOREPOXIDEJ /2 NA METHOXYCHLOR NA ENORIN KElONE 16 PERCENT MOISTURE
• • • ... ..
•• • • ..
•••FOOTNOTES••• •A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-EST!MATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWIJ TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN 10 BE GREATER THAN VALUE G!VW •U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM OUAIHITATION LIMIT. C-CONFIRMED BY GC/MS
1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-
------ --- -
SAMPLE AND AIJALYSJS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA.
PEST!CIDES/PCB'S DATA REPORT • • • ,. ·········••*••·······"'•*•·"'**' PROJECT NO. 90-785 SAMPLE NO. 48900 SAMPLE TYPE: SOIL SOURCE: CAROLINA TRANSFORMER
• • •
- -- --
"' • • • • • • • • * • • .. .. .. STATION ID: 6-SLB
PROG ELEM: SSF CITY: FAYETTEVIL COLLECTION START:
COLLECTED BY: D THOMAN ST: NC 08/07/90 1130 STOP: 00/00/00
UG/KG AIJALYTICAL RESULTS l_lG/KG ANALYTICAL RESULTS
NA ALDRIN 190U PCB-1232 (AROCLOR 1232)
NA HEPTACHLOR 190U PCB-1248 ( AROCLOR 1248)
NA HEPTACHLOR EPOXIDE 190U PCB-1260 ( AROCLOR 1260)
NA ALPHA-BHC 1 !,JOU PCB-1016 (AROCLOR 1016)
NA BETA-BHC NA TOXAPHENE
NA GAMMA-BHC (LINDANEl NA CHLORDENE /2
NA DELTA-BHC NA ALPHA-CHLORDENE /2
NA ENDOSULFAN I ( ALPHA) NA BETA CHLORDENE /2
NA DJELDRIN NA GAMMA-CHLORDENE /2 NA 4,4'-DDT lP.P'-DDT) NA 1-HYORL)XYCHLORDENE /2
NA 4,4'-DDE (P.P'-DDE) NA GAMMA· Cl ILORDANE /2 NA 4,4'-DDD (P,P'-DDD) NA TRANS-NONACHLOR /2 NA ENDRIN NA ALPHA-CHLOROANF /2
NA E~JDOSULF AN I I (BETA) NA CJS-NONACHLOR /2
NA ENDOSULFAN SULFATE NA OXYCHLORDANE (OCTACHLOREPOXIDE) /2
NA CHLORDANE (TECH. MIXTURE) /1 NA METHOXYCHLOR
190U PCB-1242 (AROCLOR 1242) NA ENORIN KETONE
190U PCB-1254 (AROCLOR 1254) 7 PERCENT MOISTURE
190U PCB-1221 ( AROCLOR 1221 l
.. , •REMARKS"*•
-09/19/90
• • • .. . .. .. .. ..
•••FOOTNOTES•*• •A·-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERE~JCES •J-EST!MATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •~.-ACTUAL VALUE IS KNOWIJ TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS ~.NOWN TO BE GP.EATER THAN VALUE GIVEIJ •U-MATERIAL WAS ANALYZED FOR ~UT NOT DETECTED. THE IJUMBER IS THE MIIJIMUM QUANTITATJON LIMIT. C-CONFIRMED BY GC/MS 1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OP. METABOLITES OF TECHIJ!CAL CHLORDANE.
-
-- - ----
PEST!CIDES/PCB'S DATA REPORT
- --- -
SAMPLE AND AIJALYSJS MANAGEMENT SY5TEM
EP.il.-REG!O~l 11.1 ESD. ATHEtJS. GA. - ----
..
••
" • •
PROJECT NO. 90-785 SAMPLE
SOIJRf,F: f:ll.R:()L I W\ TR.i\NSFORf.1ER STATION ID: 7-SLh
NO. 48917 SAMPLE TYPE: SOIL PROG ELEM: SSF COLLECTED CITY: FAYtTTEVIL
COLLECTIOtJ START: 08/07/90
BY: D THOMAN
ST: NC
1450 STOP: 00/00/00
1..!G/Y.C Ai,iAL'i'TICAL RESULTS ANALVT!Cr"-.L
tJA ALDRIN 95CU PCO--i 232 ( AROCLOR 1232) N.6. H!::P rti.CHLOR 9SOU PC~-12'18 { .l\RCCLOR 1248) !.A HEPTACt1LOR EPOxlL)E 600J PCB-1260 (AROCLOR 1260) M/1, :'\U'H/'. -~IIC 950U PCB-1016 (AROCLOR 1016) NA RtlA-BHC NA TOXAPHENE NA GAMMA-BHC ( LI NDANE l NA CHLORDENE /2 '[A DEL r.t~.-BHC NA ALPHA-CHLORDENE /2 NA ENDOSULFAN l (ALPHA) ,.~ BETA l,HLuKut.Nr: /2 ~J,'\ D!E:...DRHJ NA GAMM.'\-CHLORDE~JE /2 NA 4 ,il'-[)f)I 1_ i,;,, P'-DDT) NA i -H V OR:f.>X VCI--ILO!'<lJt NI: /2 ~JA 4,4'-DDE (P.P"-DOEl ~J.\ GA:.~~.~:.-CHL Grt:U,\I\IE /2 NA 4.4'-DDD (P.P'-DDD) NA I~ llf\lS,-Ml_lf,!_O_t·!--!L OR /2 "~ [hiUR i N NA ALPHA-CHLOROANF /2 NA Et~OCSULF ;.JJ I I (BETA) NA CJS-NONIICHLOR /2 NA fl\JQOSl_lLf,t.N S!JLf /\ l E ;JA OXVCHI Of<[IANf: '· OCTACYL0REPOX I DE) /2 '" CHLORD~i~E (TCCM. MiXTURE i /1 NA r.~E THOX\'CI lLCR O,M
91:'.iOU PCB-1242 (/\ROCLOR 12~2) NA FNllR!N KEfONE 950U PCB-1254 (_ AROCLOR 1 2.S-4) 15 PERCENT MOISTURE 950U PCB-1221 (AROCLOR 1221)
• ._.. FOOTNOTfS• • •
-09/22/90
•• •• .. ..
TA-A'✓E:1AGE 'v'~LLlE •i-.iA-1-.iOT ANAL"v"/fD *f\lA!-!M!E.RFERE.MCES •J-ESTI~.~ATED VA:..UE :i::J-PR[S:JM,:TIVE EVIDENCE OF ~RE5ENU:'. Ut-MATERIAL •K-ACTUAL VALUE JS wow:J TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•LI-MATERIAL WAS ANALY7fD FU~ BllT NOT DETECTED. THE ~UMBER IS TIIE MIWIMUM QUANTITATION LIMIT. C-CONf1RMED BY GC/MS 1. WHEN NO VALUE IS REPORT[D. SEE CHLORDANE CONSTITUFNTS. 2. CONSTITUENTS QR METABOLITES Of TECHNICAL CHLORDANE.
-
- -- -
eESIJCIDtS/PCB'S DATA REPORT
" ••
" .. PROJECT tJO. 90·785 SAMPLE
SOURCf: r:.o.ROL INI\ TR.ti.NSFOR.MER STATION ID: 7-SLB
- -
NO. 4&918
--- - -- ----SAMPLE AND ANAL VS IS MANAGEMENT SV5TEM
EPA-P.EGIOH !V ESD. ATHeJS, GA.
PROG ELEM: SSF COLLECTED CITY: FAYETTEVIL COLLECTION START. 08/07/90
BY: D THOMAN ST: NC 1505 STOP: 00/00/00
-
U!l/22/90
••* • t + • • ~ ♦ • • • • * + ♦ * * • • • • • * • • * T * * * t t * $ • • ♦ * * ♦ ♦ * ♦ ♦ ♦ ♦ * * * * * ♦ ♦ ♦ ♦ * ♦ * T ♦ ♦• * ♦ 9 ♦ UG,'Y,G Al~1\L YT I CAL K.ESUL TS '-'G/!<.G A~JAL \'TI CAL R[~iJL TS
•• •• •• ..
IJA ALDRIN 660t.1 PCB-12:J2 (AROCLOR 1232) ~· HtPIAC~LOR 66011 PCS-12/48 (/\ROCLOR 1243) i.JA HEPTACHLOK EPUXIDE 350JN PCB-1260 ( AROCLOR 12601 ~~-" .".:... ;'f-'::'\ 3!tC 660U PCB-1016 (AROCLOR 1016) NA AUA-BHC NA TOXAPHENE NA GAMMA-DHC ( LINDANE) NA CHLDRDENE /2 NA DEL T.ti.-BHC NA ALPHA-CHLORDENE /2 NA ENDDSULFAN l ( Al PHA) "~ BETA CHLORDi:NF. /2 ~JA CIELCR.lt4 NA GAMMA-CHLORDD4E /2 NA 4 .a•-rinr (P,P'-QC'T) NA i -HY(ll<(1x YCHLORD!-:Nt /2 t" 4:4"-DDE (P.P'-DDEI W\ GAl.~MA--Cl·lLGRD,\l,JE /2 ,~
N• 'l.4'-DDD ( P. P • -DDD) NA 1 I? Al\1$-~!(l~J.A.•.:HL QR 10 i-.iM. i::NDR i i..j NA ALPHA-CHLOROANF /2 ~J,'\ E~~DOSUL.F AN I I (SETA) NA CJS-NONACHLOR /2 NA fN00~1.ILF.AM S1_1Lr.~.1 E NA OK VCHI ORllANt: fOCTACHLOREPOXJDE) /2 IJA CHLORD,"-t,JE (T[CH. 1.iIXTuRE) /1 NA ME THOXYCI ILOR bbOU PCB-1242 (AROCLDR 1242) NA FNORJN HTONE 660U PCB-1254 < AROCLOR I ?54) , .0 PERCENT MOISTURE 660U PCB-1221 (AROCLOR 1221)
•••FOOTNOTES•••
'tA-A'v'ER,!.GE 'v'ALUE •l-.iA-1,JOT ANM.L'v'/FD •~Al-!MIERfEREMCES •J-ESTIMATED VALUE •N-PR[Slirv!PTIVE EVIDENCE OF PRESENCI: U!-' MATERIAL •r-•CTUAL VALUE IS /".tJOW:J TO BE LESS THAIJ V~LUE GIVEN •L-ACTUAL VALUE IS SNOWN TO BE GREATER THAN VALUE GIVEN
•LI-MATERIAL WAS ANAl..v'7f:f) FOR tjl,IT MOT DETECTED. THE mmSER IS THE MHJ!MliM QUAIHITATION LIMIT. C-CONFIRMED BY GC/MS ~. WHnJ tm VALUE rs REPCRT[O, SEE CHLORDANE CONSTITUF.NTS. L. CONSTITL'ENTS OR METABOLITES Of TECHtJICAL CHLORDANE.
-
-·---- - -- - - - - - - - - - -
PESTICIOES/PCB'S DATA REPORT
SAMPLE ANO ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA.
••• • • • • • • • • • • • • • * •••••• *. * * •• * • * • • • • • • • * • • • * " • • • • • • • • * • • • • • • * • •• PROJECT NO. 90-785 SAMPLE NO. 48919 SAMPLE TYPE: SOIL • • SOURCE: CAROL I NA TR.ANSFORMER •• STATION ID: 8-SLA .. PROG ELEM: SSF CITY: FAYETTEVIL COLLECTION START:
COLLECTED BY: D THOMAN
ST: NC 08/07/90 1440 STOP: 00/00/00
09/19/9D
• • • ... .. .. .. .. ♦.i.+ ♦ + .f • • • • ♦ • ♦ • ♦ * ♦ * • * * • * • • ♦ ♦ T ♦ ♦ :J ♦ * T ♦ .j. • • ♦ ♦ ♦ * • ♦ ♦ • ♦ ♦ ♦ * * ♦ ♦ ♦ * ♦ ♦ * • 1' • • * ♦ * *** UG/r,G A/JAL YT I CAL RESULTS UG/r.G ANAL YT! CAL RESULTS
N~ ALDRIN 840U PCB-1232 (AROCLOR 1232) NA Hl:PTACHLOR 840U PCB-1248 (AROCLOR 1248) NA HEPTACHLOR EPOX IDE 4800 PCB-1260 ( AROCLOR 1260) NA At..PHA-BHC 840U PCB-1016 (AROCLOR 1016) NA BETA-BHC NA TOXAPHENE NA GAMMA-BHC ( LI NOANE l NA CHLORDENE /2 NA DELTA-BHC NA ALPHA-CHLORDENE /2 NA El<DOSULFAN I (ALPHA) NA BETA CHLORDENE /2 . NA D!ELDRIN NA GAMMA-CHLOROEtJE /2 NA 4,4'-DDT ( P. P' -DDT) NA 1-HYOROXYCHLORDENE /2 NA 4.4"-DDE (P.P'-DDE) NA GAMMA-CHLORDANE /2 NA 4,4'-DDD (P.P'-000) NA TRANS-NONACHLOR /2 NA [NORIN NA ALPHA-CHLOROANF /2 NA EtJOOSULFAN II (BETA l NA CIS-NONACHLOR /2 NA fNDOSULFMI SULFATE NA OXYCHLOROANE (OCTACHLOREPOXIDE) /2 NA CHLORDANE (TECH. MIXTURE) / 1 NA METHOXYCHLOR 840U PCB-1242 (AROCLOR 1242) NA FNORIN KETONE 4500U PCB-1254 (AROCLOR 1254) 11 PERCENT MOISTURE 840U PCB-1221 ( AROCLOR 1221 l
••*REMARKS••*
•••FOOTNOTES•••
•A··AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWN TO BE LESS THA/J VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN •LI-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. C-CONFIRMED BY GC/MS
1. WHW NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-
----- - - ---- - -- -- -
Pt~l!CIDES/PCB'S DATA REPORT
" .. .. ..
+ • • • • • • • • • • • • • • • • • • •
PROJECT !JO 90· 785 SAMPLE NO. 48920
SOURCf: · CAROLINA TR.ti,~JSFOP.MER STATION ID: 8-SLB
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EP,n.-REG!OM IV ESD. ATHEt~S. GA.
*****1'TT1'* 4'.i;.j,+••""·"'················ SAMPLE TYPE: SOIL PROG ELEM: SSF COLLECTED CITY: FAYETTEV!L CCLLECTIO:J START: 08/07/90
BY: D THOMAN ST: NC 1455 STOP: 00/00/00
--
UW22/90 ...
•• •• • •
♦++ ~ + + • • + • • * * * * * * + * • • • • • • • • • t • • * T * i * * + + • * • * * * • • IJ * • * * * * • * • * • • * * T t T T1'* UG/KG ANALVTIC~L RESULTS UG/~G ANALYTICAL RESULTS
!IA ALDRHJ $$OU F'CB-·1232 (AROCLOR 1232) NA HE.PIACHLOR 61-)0U PCB-12'18 (AROCLOR 1248) i,A HEilTACHLOR EPOX!UE 1100 PCB-1260 (AROCIOR 1 ~fiO l ~Y'. :'\~_.:.'}!.'\· B: lC 660U PCB-1016 (AROCLOR 1016) NA BUA-BHC NA TOXAPHENF. NA GAMMA-BHC ( L!NDANE) NA CHLORDENE /2 NA DELT.ti.-BHC NA AL~HA-CHLORDENE /2 NA ENDOSULFAN I ( ALPHA) N" 6ETA CHLOROFNE /2 ~ NJ'. 01ELDRitJ NA GAMMA-CHLORDENE /2 NA .d ll' -!'l!Jf 1,P. P' -DDT) NA 1-H'll.)Rt"lXYCl-iLOROE:Mf /2 NA 4:4·-GDE (P.P'-DDE) W", GAMMA-CHLORDAfJE /2 N~ 4.4'-DDD (P, P' ··DDDJ NA I RAl\l'S-M(lM.fJ..1.:HLOR M
i~M D..iDR. IN IJA ALPHA-CHLORnANf' /2 N,~ EtmOSULF,!UJ I! (BETA) NA CIS-NONACHLOR /2 NA f:NOOSIILF.ll.N SIJ!....f/\TE NA OXVC.HI .11RLIANI: ( OCT ACHLOREPOX IDE) /2 rJA CHLCRDAiJE (TECl-i. MiXTURE) /1 ~JA METHOXYCIILCR 6b{1U PCB-1242 ( IIROCLOR '. 242) NA fNllR!N •ETONE lOOOU PCB-1254 ( AROCLOR 1254 J 6.3 PERCENT MOISTURE 650U PCB-1221 (AROCLOR 1221)
•••REMARKS•••
•••FOOTNOTES•••
-tA-AVERAG[ VALVE •i-JA-NOT ANALY/FO •N;.l-!NIERf!:RENCES •J-ESTIMATEO VALUE •rJ-PR[SUMPTIVE EVIDENCE OF Pr<ESENLI: Ot-MATERIAL •r,-•CTUAL VALUE IS r,NOW!J TO BE LESS THAN VALUE GIVEN •L-ACTUA!. VALUE IS •NOWN TO BE GREATER THAN VALUE GIVEN
+U-MATERIAL WAS ANAI.Y7F:fl FU!-? ~I.IT MOT DETECTED. THE WJMBER IS THE MirnMUM QUAI-JTITATION LIMIT. C-CONFIRMED BY GC/MS 1. WH~ll NO '✓ALUE IS REPORTCD, SEE CHLORDANE CONSTITUFNb 2. COf!STITL'HJTS OR METABOLITES OF TECHIJ!CAL CHLORDANE.
-
------------------PEST!CIOES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. ... .. .. .. ..
• • * • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • PROJECT IJO. 90-785 SAMPLE NO. 48915 SAMPLE TYPE: SOIL SOURCE: CAROL INA TRANSFORMER STATION ID: 9-SLA
PROG ELEM: SSF COLLECTED CITY: FAYETTEVIL COLLECTION START: 08/07/90
BY: D THOMAN ST: NC 1255 STOP: 00/00/00
-
09/19/90
• • • .. . .. .. ..
• •
••• + ♦• ♦ • ~ ••••••••••••••••••• * •• * •• * ••••••••••••••••••••••••••••••••• UG/KG AIJALYTICAL RESULTS lJG/KG ANALYTICAL RESULTS NA ALDRIN 190U PCB-1232 ( AROCLOR 1232) NA HEPTACHLOR 190U PCB-1248 (AROCLOR 1248) NA HEPTACHLOR EPOXIDE 260U PCB-1260 ( AROCLOR 1260) NA ALPHA-BHC lsJDU PCB-1016 (AROCLOR 1016) NA BETA-BHC NA TQXAPHENE NA GAMMA-BHC (LINDANE) NA CHLORDENE /2 NA DELTA-BHC NA ALPHA-CHLORDENE /2 NA ENDOSULFAN I (ALPHA) NA BET A CHLORDENE /2 NA DIELDRIN NA GAMMA-CHLORDENE /2 NA 4,4'-DOf (P.P'-DDTJ NA 1 -HYOROXYCHLORDENF /2 NA 4,4'-DDE CP.P'-DDEl NA GAMMA· CHLOROA:JE /2 NA 4,4'-DDD (P,P'-ODD) NA TRANS-NONACHLOR /2 NA [NORIN NA ALPHA-CHLORnANf /2 NA rnooSULFAN II ( BETA) NA CIS-NONACHLOR /2 NA ENDOSULFAN SULFATE NA OX YCHLORUANE ( OCTACHLOREPOXIDE J /2 NA CHLORDANE (TECH. MIXTURE) /1 NA METHOXYCHLOR 190U PCB-1242 (AROCLOR 1242) NA FNnRJN KETONE 2GOU PCB-1254 (AROCLOR 1254) 11 PERCENT MOISTURE 190U PCB-1221 ( AROCLOR 1221)
,.... • FOOTNOTES• n •A··AVERAGE VALUE •NA-NOT ANALYZED •NAI-JNTERFERENCES •J-ESTJMATEO VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE JS r-NOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS ,.NOWN TO BE GREATER THAN VALUE GIVEN •U-MATERIAL WAS ANALYZED FIJK tlllT NOT DETECTED. THE NUMBER IS THE MIIJIMUM QUANTITATION LIMIT. C-CONFJRMED BY GC/MS 1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-
-------
PE~11I:totS/PCB'S DATA REPORT
-----SAMPLE AND ANALYSIS MANAGEMFNT SYSTEM EPA.-REG!OM IV ESD. ATHENS, CA.
------
O!,J/22/90 ••• 4 4 * • • * • S • * * * S $ * * • • * t t t •. • TT TT $ * * *. * ♦ 4 • * * * •••••••••••••••••••••••• ,. PROJECT NO. 90·785 SAMPLE NO. 48916 SAMPLE TYPE: SOIL PROG EL EM: SSF COLLECTED BY: D THOMAN • • • • SOURC:f: C:A_ROL I NA TR.lli.NSFOR~~ER CITY: rAYETTEVIL ST: NC " ,, STATION ID: 9-SLB COLLECTIOtJ START: 08/07/90 1300 STOP: 00/00/00 •• .. 4 •• ♦ 4 ~ + + ~ 4 • • * * 4 $ 4 $ * t * t $ * t • $ t • ~ * * $ l l * 4 4 * * * * * * * * 4 • * * S * S S S S t St$ t •• St ••• UC/KC Af,JAL','iICAL RC:SULTS l.tr.:i/KG ,'!.tJA:...'.'TICAL r:c~ULTS
tJA ALDRIN 52OU PCB--1232 (AROCLOR 1232) NA H!:PIACHLOR 52()1J P•:B-12'18 ( AROCLOR 1248) i-JA HEPTACHLOR EPOX !Dt 520U PCB-1260 ( AROr.t.nR 1?60) ~~!\ /1.LP!iA SHC 520U PCB-1016 (AROCLOR 1016) NA BUA-BHC NA TOXAPHENE NA GAMMA-OHC ( LI NDANE) NA CHLORDENE /2 'IA DELTA-BHC NA AL~HA-CHLOHDENE /2 NA ENOOSULFAN J (ALPHA) "k BETA CHLORDENE /2 N:'\ DJELDRIN NA GAMfl..~-CHLORDENE /2 NA 4 .a· -nor (D.P'-Qf:T) NA 1-Hvt)R:0.X v,_.HLOR(lfl..J!: /2 tJA 4 ·.~'-DOC (P.P"-DDEl rJ~ GAMMA-CHLGRD/,i>JE /2.. NO 4,4'-DDD ( r. P' ·DDD) NA 'fk AMS-Nl:l~J.fl_(!-!!.. OR /2 j.,j~ Li..iU;;:IN NA ALPHA-CHLOROANF /2 ~!A flJDOS~LF AN I I iBETA) NA CI S-NmJACHLOR /2 NA f ND051JL F A."J SU!..F:\TE NA OX YCHl_(JRUANE ( CIC T AGHLQREPOX !DE) /2 NA CHLORDHNE (TLCH. MIXTURE) / I ~~/'. METHOXYCI !LOR 5'2'JU P(B-1242 ( AROCl.OR 1242) NA FNOR IN K.1:TONE S20U PCB-1254 ( AROCLC1R 1254) 7.5 PERCENT MOISTURE 520U PCB-1221 ( AROCLOR 1221)
•••FOOTNOTES•••
,-A-AVERAGE VAL.LlE •l..iA-NUT ANAL"v"/fi"J • AJ-1"l1ER~EREMCES •.!-ESTIMATED VALUE *fJ-?RESUMPTIVE EVIDENCE OF ~RESENCI:: UI-MATERIAL •K-llCTUAL VA!...L'E IS KNOWN TO BE LESS THAN •LI-MATERIAL WAS ANAl.V2f0 FU~ BUT NOT DETE 1 . WHe! NO VALUE rs REPORT[D. SEE CHLORD
ALUE GIVEN •L-ACTUAI VALUE IS KNOWN TO BE GP.EATER THAN VALUE GIVEN TED. THE ~JW.mER IS THE MHJIMUM QUAi.JTITATION LIMIT. C-('ONFIRMED BY GC/MS NC CONST I TuFNTS 2. r::ONSTI TUENTS OR METABOLITES OF TECHtJICAL CHLORDANE.
-
-·---------- -- - - - -
PtSfJCJOtS/PCB'S DATA REPORT
SAMPLE AIJD ANALYSIS MANAGEMENT SYSTEM
EP/l.-P.EGION IV ESD. ATHEfJS, CA. ... ♦ ♦ ♦ f a ♦ , • • • * * * * $ • • * * * T * * * T T ~ ~ ~ * " .. .. .. PROJECT NO. 90-785 SAMPLE NO. 48913 SAMPLE TYPE: SOIL SOURU:: CAROL IN/I TP.P..~JSFORMER STATION ID: 10-SLA
Ai-./MLVTICAL RESULTS
NA ALDRIN NA HEPfACHLOR NA HEl'TACHLOR EPOXJDE W\ 111 r, 11 I\ D' ,,-..... , ',,.,. u,,..., NA AtlA-BHC NA GAMMA-□HC ( LI NDANE) MA DEL Tti.-BHC NA ENDOSULFAN I ( ALPl-iA)
W\ D!ELDRIIJ NA 4, 4, -•-1u r (D P'-nnTl
N:.. 4,4'-DDE (p:p -DDEl
NA 4,4'-DDQ (P.P'-DDD) i~M. LhiUr\IN ~JA ENDOSULf AiJ I I (BETA) NA Ft,.J[l051.ILF .A.M SULr/\lE NA CHLCRD/~/JE (TLCH. MDTURE l /I
~{11}\J PCB-1242 ( AROCLOR 1242) soou PCB-1254 (AROf.LOR 1 25.£1) 500U PCS-1221 (AROCLOR 1221)
• • • FOOTNtlTES•• •
' . ' ♦ • ♦ • ' ' • • • • • • • • • • • • • • • • • • • • PROG ELEM: SSF CITY: FAYETTEVIL COLLECTED
COU ... ECTimJ START; 08/07/90
BY: D THOMAN ST: NC
i215 STOP: 00/li0/00
"""' \/TTf'•• ,..,,-,..,,. ~--,..,,~,....._ o I J..._,Ml-"LJVL I _=i
500U PCB-1232 (AROCLOR 1232) soou PCB-12/48 ( AP.OCLOR 1248) /400JN PCB-1260 ( AROr.LOR 12(;0) 500IJ PCB-1016 ( AROCLOR 1016) NA TOXAPHENE NA CHLORDENE /2 NA ALPH.A-CHLOKDENE /2
O,M DETA CHLORlJF.NE /2 NA GAMMA-CHLORDEt~E /2 NA 1-HYiJ~Ox YCHLU~Oft..Jf /2 tJA GAMMM-CHLOROAi~E /2 NA I N'AI\IS-~!OM.a.t·H!....OR ,..,
NA ALPHA-CHLORnANF /2 NA CIS-NON/ICHLOR /2 NA O)(YCHI OkLlANE <. OC f M'.HLOREPOX IDE) /2 W\ METHOX\'Ct !LOR NA FNnRIN KE fONE 12 P[RC[IH MOISTURE
-
0!,/22/90 . . ' . .. •• ..
• •
TA-AVERAGE VAUJE +i.JA-hiOT ANAL"v?FD •N.o.I-1"'!1ERFEP.ENCES •J-ESTn.~ATED VALUE •:~-~R[St.:iwiri!VE EVIDENCE Of PRESENCC Uf MATERIAL •K-ACTU~.L VALUE IS nJOWIJ TO BE LESS THAIJ VALUE GIVEN •L-ACTUAI VALUE IS rnOWN TO BE GP.EATER THAN VALUE G!VEIJ •U-MAiERIAL WAS ANAi Y~Fn Fu~ BllT NOT DETECTED. THE NUMBER IS TllE MINIMUM OUANT!TATION LIMIT. C-CONFIRMED BY GC/MS
1. W~E~J ~m VALUE IS REPORT[G, SEE CHLORDANE CONSTITUFNTS. 2. C0NST!Tl1ENTS OR ~-~ETABOLITES OF TECHf..JICAL CHLORDANE.
-
~
- - -
PESTICIDES/PCB'S DATA REPORT ••"-• .......... *••••t:•• •• PROJECT NO. 90-785 SAMPLE • • SOURCE: CAROLI NA TRANSFORMER " STATION ID: 11-SLA ..
- -- - - - - - -- - -
• • • • • NO. 48903
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS. GA.
SAMPLE TYPE: SOIL PROG ELEM: SSF COLLECTED CITY: FAYETTEVIL
COLLECTION START: 08/07/90
BY: D THOMAN ST: NC 1100 STOP: 00/00/00
-09/19/90
♦♦♦ ♦ ♦ ♦ ♦ ♦ ••••••• * • * ••••••••••• * * * * • * •••••••••••••••••••••••••••••••••
UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS
NA ALDR!t. 11 oou PCB-1232 ( AROCLOR 1232) NA HEPTACHLOR 1100U PCB-1248 lAROCLOR 1248) NA HEPTACHLOR EPOX IDE 4800 PCB-1260 (AROCLOR 1260) NA ALPHA-BHC 11 oou PCB-1016 (AROCLOR 1016) NA BETA-BHC NA TOXAPHENE NA GAMMA-BHC ( L!NDANE) NA CHLORDENE /2 ~IA DELTA-BHC NA ALPHA-CHLORDENE /2 NA ENDOSULFAN I ( ALPHA) NA BETA CHLORDENE /2 NA D!ELDRIN NA GAMMA-CHLORDENE /2 NA 4,4'-0DT lP.P'-DDT) NA 1-HYUROXYCHLORDENE /2 NA 4.4'-DDE (P.P'-DDE) NA GAMMA ··Cl iLORDAIJ[ /2 NA 4.4'-0DD (P.P'-DDD) NA TRANS-NONACHLOR /2 NA CNDRIN NA ALPHA-CHLORDANE /2 NA ENDOSULF All I I (BETA) NA CJS-NONACHLOR /2 NA ENOOSULFAN SULFATE NA OXYCHLORDANE tOCTACHLOREPOXIDE) /2 NA CHLORDAIIE ( TECH Ml XTURE) /1 NA METHOXYCHLOR 1 lOOU PCB-1242 (AROCLOR 1242) NA cNORIN KETONE 4500U PCB-1254 (AROCLOR 1254) 12 PERCENT MOISTURE 1100U PCB-1221 lAROCLOR 1221)
, nREMARKSn•
•••FOOTNOTES*•• •A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-EST!MATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEIJ •U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATJON LIMIT. C-CONFIP.MED BY GC/MS 1. WHEIJ NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-
------- -- - - - - - -- --
PESTICIDES/PCB'S DATA REPORT
SAMPLE AIJD ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD. ATHENS. GA. .. .. .. ..
............................ **••······ PROJECT NO. 90-785 SAMPLE NO. 48904 SAMPLE TYPE: SOIL SOURCE: CAROLINA TRANSFORMER STATION ID: 11-SLB
UG/r,G ANALYTICAL RESULTS
IJA ALDRIN NA HEPTACHLOR
NA HEPTACHLOR EPOX!DE NA ALPHA-BHC NA BETA-BHC
NA GAMMA-BHC (LINDANE) NA DELTA-BHC NA ENDOSULFAN I ( ALPHA)
NA DIELDR!IJ NA 4,4'-0DT (P.P'-DDT) NA 4.4'-DDE (P.P'-DDEl NA 4.4'-DDD (P.P'-DDD) IJA ENDRIN NA EtJDOSULF AN I I (BETA) NA ENDOSULFAN SULFATE IJA CHLORDANE (TECH. MIXTURE l / 1 210U PCB-1242 (AROCLOR 1242) 300U PCB-1254 (AROCLOR 1254) 210U PCB-1221 C AROCLOR 1221)
•••FOOTNOTES•••
• • • • • • • • • • • • • • • • • • • • • • • • •• . COLLECTED BY: D THOMAN PROG ELEM: SSF CITY: FAYETTEVIL COLLECTION START: ST: NC 08/07 /90 1120 STOP: 00/00/00
ANALYTICAL RESULTS
210U PCB-1232 CAROCLOR 1232) 210U PCB-1248 (AROCLOR 1248) 330 PCB-1260 (AROCLOR 1260) 210U PCB-1016 (AROCLOR 1016) NA TOXAPHENE NA CHLORDENE /2 NA AI_PHA-CHLORDENE /2 NA BETA CHLORDENE /2 NA GAMMA-CHLORDEIJE /2 NA 1-HYllf<OXVCHLORDfNE /2 NA GAMMA--CHLOROAIJE 12 NA TRANS-NUNACHLOR /2 NA ALPHA-CHLOROANf 12 NA CIS-NONACHLOR /2 NA OXYCHLORDANE (OCTACHLOREPOXIDE) /2 NA METHOXYCHLOR NA fNORIN KETONE 6 PERCENT MOISTURE
-09/19/90
• • • ... •• .. .. ..
•A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-EST!MATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWIJ TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN •U-MATER!AL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. C-CONFIRMED BY GC/MS 1. WHEIJ NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-
--·-- - - ------- ---- -
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD. ATHENS. GA. ... .. .. .. ..
• * ••• "'"'**". *"** ······•***"*** * • • • * * * • * * * * * * * * * * * • * * * * • * * * * • PROJECT NO. 90-785 SAMPLE NO. 48903 SAMPLE TYPE: SOIL SOURCE: CAROLINA TRANSFORMER STATION ID: 11-SLA
PROG ELEM: SSF CITY: FAYETTEVIL COLLECTION START:
COLLECTED BY: D THOMAN ST: NC 08/07/90 1100 STOP: 00/00/00
09/19/90
• • • ... .. .. .. ..
+++ + + + + • +. *. *. * * * * * * * * * * * * *. * * * * * • * * • * * * * * * * * * * * * * * * * * * * * * *. *. * * * ••• UG/KG ANAL YT !CAL RESULTS UG/KG ANAL YT!CAL RESULTS
NA ALDRIIJ 11 oou PCB-1232 (ARDCLDR 1232) NA HEPTACHLDR 11QOU PCB-1248 (AROCLOR 1248) NA HEPTACHLOR EPOX!DE 4800 PCB-1260 (ARDCLOR 1260) NA ALPHA-BHC 1100U PCB-1016 (AROCLOR 1016) NA BETA-BHC NA TOXAPHENE NA GAMMA-BHC (LINDANE) NA CHLORDENE /2 NA DELTA-BHC NA ALPHA-CHLORDENE /2 NA Ei<DOSULFAN I ( ALPHA) NA BETA CHLORDENE /2 NA DIELDRIN NA GAMMA-CHLORDENE /2 NA 4,4'-DDT lP.P'-DDT) NA 1-HYOROXYCHLORDFNF /2 NA 4,4'-DDE (P,P'-DDE) NA GAMMA Cl ILORDAIJ[ /2 NA 4,4'-DDD (P.P'-DDD) NA TRANS-NONACHLOR /2 NA CNDRIN NA ALPHA-CHLORllANI' /2 NA ENDOSULFAN II (BETA) NA CIS-NONACHLOR /2 NA ENOOSULFAN SULFATE NA OXYCHLORDANE lOCTACHLOREPOXIDE) /2 NA CHLORDAIJE (TECH. MIXTURE) /1 NA METHOXYCHLOR 1100U PCB-1242 (AROCLOR 1242) NA FNOR IM KET ONE 4500U PCB-1254 (AROCLOR 1254) 12 PERCENT MOISTURE 1100U PCB-1221 ( AROCLOR 1221)
•••FOOTNOTES•••
•A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWN TO BE LESS THAIJ VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN •U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTJTATION LIMIT. C-CONFIRMED BY GC/MS
1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-
--·-· ----PESTICIDES/PCB'S DATA REPORT -----SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD. ATHENS. GA.
-----... .. •• .. ·····•*•*•*•········ • • • • • • • • • • • • • • .. • • * • • • ****••············ PROJECT NO. 90-785 SAMPLE NO. 48901 SAMPLE TYPE: SOIL SOURCE: CAROL I NA TRft.NSFORMER STATION ID: 12-SLA ••
PROG ELEM: SSF CITY: FAYETTEVIL COLLECTION START:
COLLECTED BY: D THOMAN ST: NC 08/07/90 1020 STOP: 00/00/00
-
09/19/90
• • • ...
•• .. .. .. ••• ♦ ♦ ♦ ♦ •••••••••••••• * ••••••••••••••••••••••••••• * •••••••••••••••••• UG/KG ANALYTICAL RESULTS 1.IG/KG ANALYTICAL RESULTS NA ALDRIN
3200U PCB-1232 ( AROCLOR 1232) NA HEPTACHLOR
3200U PCB-1248 (AROCLOR 1248) NA HEPTACHLOR EPOXJDE 260000 PCB-1260 ( AROCLOR 1260) NA ALPHA-BHC
3200U PCB-1016 (AROCLOR 1016) NA BETA-BHC
NA TOXAPHENE NA GAMMA-BHC (LJNDANE) NA CHLORDENE /2 NA DELTA-BHC
NA ALPHA-CHLORDENE /2 NA ENDOSULFAN I (ALPHA) NA BETA CHLORDENE /2 NA DJELDRIN
NA GAMMA-CHLORDENE /2 NA 4.4'-DDT (P.P'-DDTJ NA 1-HYDROXYCHLORDENE /2 IJA 4.4'-DDE (P.P'-DDEJ NA GAll.\lA--CHLORDANE ; '2 NA 4,4'-DDD (P,P'-DDDl NA TRANS-NONACHLOR /2 NA [NORIN
NA ALPHA-CHLOROANE /2 NA ENDOSULFAN II (BETA) NA CJS-NONACHLOR /2 NA ENDOSULFAN SULFATE NA OXYCHLOROANE (OCTACHLOREPOXIDEJ /2 NA CHLORDANE (TECH. MIXTURE) /1 NA METHOXYCHLOR 3200U PCB-1242 (AROCLOR 1242) NA FNOR!N KETONE 250000U PCB-1254 (AROCLOR 1254) 11 PERCENT MOISTURE 3200U PCB-1221 ( AROCLOR 1221)
•••FOOTNOTES•••
•A-AVERAGE VALUE •NA-NOT ANALYZED •NA!-INTERFERENCES •J-EST!MATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE JS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN •U-MATER!AL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MW!MUM OUANTITATION LIMIT. C-CONFIRMED BY GC/MS
1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-
-·---- - -- - ----- - --
PEST!CIDES/PCB'S DATA REPORT ••• .. .. .. ..
• • • • • * • • • • • * * • *
PROJECT NO. 90-785 SAMPLE
SOURCF. : CAROL I ~JA TRANSFORMER STATION ID: 12-SLB
• * • .. ..
NO. 48902
• • • • • • • • * * • .. ..
UG/Y-G
fS:A NA NA
~.!l\ NA NA NA NA
N,'\ NA
TJA NA
i,,iA
WI NA
NA
AIJAL VT! CAL RESULTS
ALDRIN Ht:P!ACHLOR riEPTACHLOR EPOX!DE
.'\LPHA·-B: :c Bt:T A-BHC GAMMA-BHC (LINDANE) DEL TA.-BHC ENDOSULFAN I ( Al PHA) DIELDR!N 4.4'-!Jlll tP.P'-DDTJ 4.4"-DDE (P.P'-DDEl 4,4"-DDD (P,P'-DDD)
Lh.iLIRiN
EtJDOSULFAtJ II {BETA) ENOOSULFAN SULFATE
5(10!}
550000 SOOIJ
CHLORDANE (TECH. MIXTURE) /1 PCB-1242 (AROCLOR 1242) PCB-1254 (AROCLOR 1254) PCB-1221 ( AROCLOR 1221 l
• • • FOOHJOTF.S• • •
SAMPLE AIJD ANAL VS IS MANAGEMENT SYSTEM
EP.6.-P.EGION II! ESD. ATHENS. CA.
* * * * T T T T T *
SAMPLE TYPE: SO!L * • * • ........ * ............... .
PROG ELEM: SSF CITY: fAvETTEV!L COLLECTION START:
COLLECTED BY: D THOMAN ST: NC 08/07/90 1035 STOP: 00/00/00
* * ... •
1.IG/!<.G
500!J
5()01.l
57000
500U NA NA NA ... "~ NA
i.A
W', NA
NA NA NA NA NA 11
···••****** A~JAl.. \'TICA:... ~[:3~L TS
PCB-1232 (AROCLOR 1232) PCB-12~8 (AROCLOR 1248) PCB-1 260 ( AROCI OR 1 WO l PCB-1016 (AROCLOR 1016) TOXAPHENE
CHLORDENE /2 ALPHA-CHLORDENE /2 BETA CHLORDENE /2. GAMMA-CHLORDENE /2
i-H"v"Lll<(l}(V(,HLUR'DENt /2
GA~.~~t.A--Ci·iLGRD,\i~E /2
1 F(tJ.M';,-Ml_lM.ll.CHLOR /2
ALPHA-CHLOROANF /2 CIS-fJON~CHLOR /2
Oi<YCHI fJ~lJONE (OCTA!'HLOREPOXIOE) /2
METHOXYCI lLOR
l'NIJS l N KU ONE PERCENT MOISTURE
-09/22/90 ... ..
•• • • .. ...
TA-A' ... 'ERAGt VALUE .ti-.iA-NOT ANALYZFr, •MD.1-HJ'IERFERENCES •J-ESTIMATED VALUE :sf,l-PR[SUMPTIVE EVIDENCE OF PRESENCE ur MATERIAL •K-ACTLIAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEtJ
•U-MATERIAL WAS ANALVlfO Foe ~UT NOT DETECTED. THE fJUMBER IS TIIE MINIMUM QUAIJTITATION LiMIT. C-CONF!RMED BY GC/MS
1. WHE~J NO VALUE IS REPCRT[O. SEE CHLORDANE CONSTITUfNTS L. CONSTITUENTS OR METABOLITES Of TECHNICAL CHLORDANE.
-
-----
PESIJCJUtS/PCB'S DATA REPORT
- -- ----SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGIO~! IV !:SD, ATHENS. CA. - --
NO. 48889 SAMPLE TYPE: SOIL PROG ELEM: SSF COLLECTED BY: D THOMAN
ST: NC CITY: fAYETTEVIL
- -
..
•• •• ••
PROJECT NO. 90-785 SAMPLE
SOURCF: CAROL IN/\ TRM!SFORMER
STATION ID: 13-SLA COLLECT Im~ START. 08/07/90 0955 STOP: 00/00/00
•*• ♦ ~ • ♦ ~ • • • * * * * * * * * * * * • * * T T T T ~ $ TT T ~ • * • • • • • • * *
UC/1',G AiJAL'i'TICAL RESULTS
1JA
~IA NA ~J!'. NA NA
NA
NA
~J:\ NA
IJA "~ i~M
ti/\
NA NA
6ti()lJ
200000U
660U
ALDRIN
HEP!ACHLOR HEr-TACHL(JR EPOXIDE
.'\U"HA -SI IC
AEIA-BHC
GAMMA-BHC (LJNDANE)
DEL T.A-BHC
ENDOSULFAN 1 I Al PHA l 'DIELDRIN -.
4,.:i'-P!)I r.D,?'-DDT)
4,4'-DDE (P.P'-DDEl 4,4'-DDD (P,P'-DDD)
LNDRIN
ENCOSULFAIJ 11 (BETA)
fNOOSULFAN SULFATE CHLORDANE (TECH. MIXTURE)
PCB-1242 (AROCLOR 1242)
PCB-1254 IAROCLOR 1254) PCB-1221 (AROCLCR 1221)
•••FOOTNOTES•••
/1
1.11~/!".G.
6€0U
6"30IJ
220000
660U NA
NA
NA
O,K
NA NA ~;:•, NA
NA
NA NA
N.'\ NA
24
A~~AL '/TI CAL
PCB··i 232 { AROCLOR i 232)
PCB-1249 { .".P.OCLOP. 1248) PCB-1260 (AROr.LOR 12fi01
PCB-1016 (AROCLOR 1016)
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE /2
PETA CHLORDfNi: /2
GAMMA-CHLORDEtJE /2
l -t-fvDK(1,11. VCHLO~UHH: /2
GAMM~-CHLGRD,\hiE /2
TW.0.1\1':,-Ml_lM.~.f.:HLOR /2
ALPHA-CHLOROANF /2
CJS-NotJACHLOR /2
,.., .. ,. ' .. ..,.,. "LJVL I.:,
(1;,('y'CH1.nl"<UANt: I_ OC f Al_~HLOREPOX IDE)
METHOXVCl :LOR FNIJRJN i<.ETONE
PERCENT MOISTURE
•••REMARKS"""
/2
-OW22/90
•• •• • • •• "'
TA-A'./Ei!AGE VALUE •i.JA-NOT ANAL"v";f.jj •Ntd-lN!ERFERE~lCES •J-ESTIMATED VALUE •t..l-PRESUM?TI\iE EVIDENCE OF P;;i:ESENt:t:: or MATERIAL
•K-ACTUAL V~.LUE JS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAt VALUE JS K.NOWN TO BE GREATER THAN VALUE GIVEN •U-MAT[RIAL WAS ANAI_Y?Fn Fr.>e BUT MOT DETECTED. THE tlUMBER IS THE MINIMUM QUANTITATION LIMIT. C-Cm!FIRMED BY GC/MS
1. WHEll NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUFNT~. 2. CONSTITIJEtlTS OR METABOLITES OF TECHtHCAL CHLORDANE
-
------ -- - ------- --
µESIICJDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EP.l~.-REGION IV ESD. ATHEt~S. CA. ...
" •• .. ..
+ + • + 4 • • • * • • * * * * • • • • * • * • • T T T T ~ * * * * ~ • • ♦ • • • • ,.. ................. ..
PROJECT NO. 90-785 SAMPLE NO. 48890 SAMPLE TYPE: SOIL SOUR~t: CAROLINA TRANSFORMER STATION ID: 13-SLB
♦+• ♦ ♦ • + ♦ ♦ •.• • • • • • * * * • * * •. * T * T * ~ * * * T ♦ UC/r,G AIJALYTICAL RESULTS
IJA ALDRIN NA ~1:P lft.CHLDR
NA HEt'TACHLOR EPOXIUE
~!:'\ /'.:...::-OM.~, ·S!lC
NA BETA-BHC NA GAMMA-BHC ( LI NDANE) NA DEL T.A-BHC NA ENDOSULFAN I ( Al PMA ~
Nt\ DIELCRIN NA 4,4'-[)(H 1.P.P'-DDT)
r.JA 4.4'-DDE (P.P"-DDEl
,JA 4.4'-DDD (P.P'-DDDJ
i~~ LNDRIN
~JA EtJDOSULF AfJ ll (BETA)
NA F N(l()SIJL F .4.M SULfATE
~JA CHLORDAliE (T[CH. MiXiURE l /1
6bOl.l PC8-1242 (AROCLDR 1242)
5SOOU PCB-1254 ( AROCLOR 1254)
660U PCB-1221 { AROCLOR 1221)
COLLECTED BY: D THOMAN PROG ELEM: SSF CITY: fAYtTTEVIL COLLECTION START: ST: NC 08/07/90 1000 STOP: 00/00/00
~ ♦ ♦ • • • • ♦ • • . . . . . . . " . . .
l\~1111 \ITT,-.AI ,...-,-111 .,..,.. l'"'\l~l"'IL. t I .l¥r\L 1,LJUL I .;J 1_1r::./!'".G
65CU F'CB--1232 ( ARDCLOR 1232 l
6'30U PCB-12118 (AROCLOR 1248)
6000 PCB-1260 ( AROCLOR 1 20n)
660U PCB-1016 (AROCLOR 1016) NA TOXAPHENE NA CHLORDENE /2 NA ALPHA-CHLORDENE /2
'"~ BETA l,MLUt\lJrt..ir: /2
M/\ Gl\MM:\-CHLORDENE /2
l,j,\ l -HY·11t<OX:Vt.~HL•JRUtMt: /2
NA GAMMA-CHLORD1\i.JE /2 NA rR AN$-MOM.4.(HL OR / '2 tJA ALPHA-CHLORDANf /2 NA CIS-NDNACHLDR /2 NA OXYt",HI l'IRLlANI: l 00 M:HL')REPOX !DE)
Nt\ METHOXYCI ILOR NA fNO~JN KElONE
16 P[RC[NT MOISTURE
/2
0,1/22/90
• • • ... .. .. .. .. ...
•"'•FOOTNOTES••• -r A-A\.'Er!.AGE VALUE • i,JA-1.;UT ANAL Y7f.0 •!'-!.0. I-HI I ERF ERENCES • J-EST IMA TED VALUE :t:~J-PR[SUMPTI VE EVIDENCE Of PRESENCE OF MATER !AL •K-ACTU.AL VALUE IS KtJOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE JS ~.NOWN TD BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANAL\i7f[l FfJ~ t,llT NOT DETECTED. THE NUMBER IS THE MH.:IMUM QUANTITATiON LIMIT. C-CONFIP.MED BY GC,'MS 1 . WHEN tJD VALUE JS REPDRTCD. SEE CHLORDANE CONST !TUFNT5. , . CONSTITUENTS OP. MET ABDL !TES OF TECHIJl CAL CHLORDANE.
-
~ "
--·---- -- ---- - -- ---SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESO, ATHENS, GA. PEST!CIOES/PCB'S DATA REPORT ... .. .. .. ..
. . . . . ' . . . . . . . . . . . . . . . . . . . . . . . .
PROJECT NO. 90-785 SAMPLE NO. 48887 SAMPLE TYPE: SOIL SOURCE: CAROL I NA TRANSFORMER
STATION ID: 14-SLA
• • • PROG ELEM: SSF COLLECTED CITY: FAYETTEVIL COLLECTION START: 08/07/90
BY: D THOMAN ST: NC 0930 STOP: 00/00/00
09/19/90
• • • ...
•• .. .. . .
••• • • ♦ ••••••••••••••••••••••• * ••••••••••••••••••••••••••••••••••••••
UG/KG AIJALYTICAL RESULTS I.JG/KG ANALYTICAL RESULTS
NA ALDRIN 3600U PCB-1232 ( AROCLOR 1232) NA HEPTACHLOR 3600U PCB-1248 ( AROCLOR 1248) NA HEPTACHLOR EPOX!DE 1 70000 PCB-1260 ( AROCLOR 1260) NA ALPHA-BHC 3600U PCB-1016 (AROCLOR 1016) NA BETA-BHC NA TOXAPHENE NA GAMMA-BHC (L!NDANE) NA CHLORDENE /2 NA DELTA-BHC NA ALPHA-CHLOROENE /2 NA ENOOSULFAN I (ALPHA) NA BETA CHLORDENE /2 NA DJELDRJN NA GAMMA-CHLOROENE /2 NA 4,4'-DDT (P.P'-ODT) NA 1 -H'YDKOX Yl.~HLORDENF. /2 NA 4,4'-DDE (P.P'-DDEl NA GAMMA-Cl ILOROAN[ /2 NA 4,4'-DDD (P,P'-000) NA TRAN~-NONACHLOR /2 NA [NORIN NA ALPHA-CHLOROANF. /2 NA EtJOOSULFAIJ II (SETA) NA CIS-NONACHLOR /2 NA ENOOSULFAN SULFATE NA OXYCHLOROANE (OCTACHLOREPOXIOE) /2 NA CHLORDANE (TECH. MIXTURE) /1 NA METHOXYCHLOR 3600\J PCB-1242 (AROCLOR 1242) NA FNORJN HTONE 1SOOOOU PCB-1254 (AROCLOR 1254) 13 PERCENT MOISTURE 3600U PCB-1221 (AROCLOR 1221 l
•••REMARKS*••
•••FOOTNOTES••• •A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWN TD BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS ~NOWN TD BE GREATER THAN VALUE GIVEN •U-MATER!AL WAS ANALYZED FUR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. C-CONFJRMEO BY GC/MS 1. WHEtJ NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS DR METABOLITES OF TECHNICAL CHLORDANE.
-
-·-·---- -- - -------- -
PESTJCIDES/PCB'S DATA REPORT ... ..
•• •• ..
............... ".
PROJECT NO. 90-785 SAMPLE SOURCE: CAROLINA TRANSFORMER STATION ID: 14-SLB
• • • • • NO. 48888
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA.
• * * • • * * * * * • • • * * • • • • * * ··••11=••····· • • • • • SAMPLE TYPE: SOIL PROG ELEM: SSF CITY: FAYETTEVJL COLLECTION START:
COLLECTED BY: D THOMAN ST: NC 08/07/90 0940 STOP: 00/00/00
09/19/90 ... .. .. .. ..
♦♦♦ ♦ + ••••••••••••• * ••• * * *. * * • * • * * * * * •• * •••• * * ••••••••• * * ••••••••• ***
UG/KG ANAL YT! CAL RESULTS I.JG/KG ANALYTICAL RESULTS
NA ALDRIN 3200U PCB-1232 ( AROCLOR 1232) NA HEPTACHLOR 3200U PCB-1248 (AROCLOR 1248) NA HEPTACHLOR EPOXIDE 19000 PCB-1260 (AROCLOR 1260) NA ALPHA-BHC 3200U PCB-1016 (AROCLOR 1016) NA BETA-BHC NA TOXAPHENE NA GAMMA-BHC (LINDANEJ NA CHLORDENE /2 NA DELTA-BHC NA ALPHA-CHLORDENE /2 NA ENDOSULFAN I (ALPHA) NA BETA CHLORDENE /2 NA DJELDRIN NA GAMMA-CHLORDENE /2 NA 4,4'-DDT (P.P'-DDTJ NA 1-HYDROX'/CHLORDfNE /2 NA 4.4'-DDE (P.P'-DDEl NA GAMMA -CHLORDAi~E /2 NA 4,4'-DDD (P,P'-DDD) NA TRANS-NONACHLOR /2 NA CNDRIN NA ALPHA-CHLOROANI' /2 NA EtJDOSULFAN II ( BETA) NA CJS-NONACHLOR /2 NA ENDOSULFAN SULFATE NA OXYCHLORDANE (OCTACHLOREPOXJDEJ /2 NA CHLORDANE (TECH. MIXTURE) /1 NA METHOXYCHLOR 3200U PCB-1242 (AROCLOR 1242) NA ENDRJN KETONE 1 sooou PCB-1254 (AROCLOR 1254) 12 PERCENT MOISTURE 3200U PCB-1221 ( AROCLOR 1221 )
•••FOOTNOTES•••
•A-AVERAGE VALUE •l•A-NOT ANALYZED •NAI-JNTERFERENCES •J-EST!MATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAI. VALUE JS KNOWN TO BE GREATER THAtJ VALUE GIVEN •U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER 15 THE MINIMUM QUANTITATION LIMIT. C-CONFIRMED BY GC/MS 1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES Of TECHNICAL CHLORDANE.
-
-·-- ---
Pt~f!UDE,/PCB'S DATA REPORT
- - --- -
SAMPLE AND ANALYSIS MANAGEMENT SVSTEM
EP.A.-REGIOM IV ESD. ATHENS, CA.
4 $ • • • * * * • * * * * * * * * • • * * • * * ~ * T ~ ~ ~
---
PROJECT JJO. 90·785 SAMPLE NO. 48885 SAMPLE TYPE: SOIL PROG ELEM: SSF COLLECTED BY: D THOMAN
ST: NC SOURr.f: C.AROL INA TR.ANSFORMER
- -
... .. .. .. •• STATION ID: 15-SLA CITY: FAYETTEVIL
C0LLECTIOt~ START; 08/07/90 0845 STOP: 00/00/00
UC/KG Ml...iHLYTICAL R[SUL TS
iJA ALDRIN 95CU PCB .. 1232 ( ,\ROCLOR 1232) NA HEP r .A.CHLO?. 9SOIJ PCB-12-18 (AROCLQR 1248) NA HEt'TACHLOR EPOXIDE 74000 PCB-1260 ( AROCI OR 1?60)
~J/\ .'\Lf': !,". ·S: IC 950U PCB-1016 (AROCLOR 1016) NA RETA-BHC NA TOXAPHENE IJA GAMMA-BHC ( LI NDANE l NA CHLORDENE /2 NA DEL T.A.-8HC NA ALPHA-CHLORDENE /2 NA ENDOSULFAN T {ALPHA) "H DC 11-i. 1...MLUKUl:Nt. /2 NA DIELDRJN N.A GAMMA-Cf-!cORDENE /2 NA a. 4• -1_lor 1• P. P'-DDT) NA j -H-1ii,i<1)x v,;HLU!-<Uf Mt: /2 IJA 4.4'-DOE (P.P'-DDEl NA c.:..r.~r.1A-Ci-:LGRD,'\i...i[ /2 NA 4.4'-DDD (P,P'-DDD) Ni>. I ~/ll\l':-,-!',-!l~lM_l)._fH!..OR 10
i...iM [hiURirJ NA ALPHA-CHLOROAt-Jf /2 ~~/\ emoSVLF AtJ i: (BETA) NA CIS-NONACHLOR /2 NA f: NDOSl.lL FAM '5'-'!....f/\1E NA OXYC'.HI. (JRL)AME (_ ocr ,O.CHLOREPOX I DE) /2 NA CHLORDAl<E { IECH. MIXTURE) ii ~J/1. METHO:{YCllLOR
9SOll 1->C~-1242 (AROCLOR 1242) NA FNORIN Kt !ONE 70000U PCB-1254 ( AROCL(IR 1?54.l 19 PERCENT MOISTURE YSOU PCS-1221 {AROCLCR 1 221 )
•••FOOTNOTES•••
-ll\J/22/90 . . ' , ..
•• .. .. ..
T A-AVEr..AG[ 'v'AU.:E • i-.iA-NOT ANAL Y7EO •"!A 1-1 NI ERF ERENCES • J-ES T IMATEC VALUE • fJ-PRCSLlM~T I VE EVi DENCE OF PRESENCI: ui-MATER !AL
•K-ACTUAL VALUE IS r-1mw1J TO BE LESS THAN VALUE GIVEN •L-ACTUAI. VALUE IS SNOWN TO BE GREATER THAN VALUE GIVEJJ
•U-MATERIAL WAS ANAi. Ylff) FU~ 8111 NOT DETECTED. THE NUMBER IS TIJE MINIMUM QUAl,TlTATION LIMIT. C-CONFIRMED BY GC/MS
1. WHrn NO VALUE IS REPORT[D, S[E CHLORDANE CONST!TUFNT5 2. CONSTITUnns OR METABOLITES OF TECHJJICAL CHLORDANE.
-
------
PESfICIOtS/PCB'S DATA REPORT ... .. •• .. ..
♦ ♦ • • • • • • • • • * • • •
PROJECT NO. 90-785 SAMPLE SOURU': CAROL I N.S TRANSFORMER
STATION ID: 15-SLB
------- --
• • * ••
NO. 48886
SAMPLE AIJD ANALYSIS MANAGEMENT SYSTEM EP.6.-P.EG!ON IV ESD, ATHEtJS, GA.
* • "' * 'f T T 1: ,t; :I:
SAMPLE TYPE: SOIL • • • PROG ELEM: SSF COLLECTED
CITY: fAYETTEV!L
COLLECTION START. OD/07/90
--
BY: D THOMAN
ST: NC
-
0855 STOP: 00/00/00
- -
09/22/90
'" .. .. ..
•• ♦♦• ♦ ♦ f f ♦ * *. S S •• * * * ••• W •• * ••• $ :j: •• * •• :j: ♦ ~ ♦ ♦ ♦ f ♦ ♦ f • ♦ * •• f • ♦ ♦ • * ••• f T 'f T * S tt•
UC/r,G AfJAL YT I CAL R.ESUL TS tJG/KG A~4A:.. ','T! CA:.. ~c:;uL TS
NA ALDR IIJ 5:JOL! PCB-·1232 (AROCLOR 1232) NA HEPTACHLOR 500U PCB-1248 (ARQCLOR 1248) NA HEPTACHLOR EPOXJDI' 760 PCB-1260 ( AROr.L OR 1 ?R())
W\ ,'\Lf'i ::.. -s:-rc soou PCB-1016 ( AROCLOR 1016) NA Bl'TA-BHC NA TOXAPHENE NA GAMMA-BHC ( LI NDANE l NA CHLORDENE /2 NA DELTA-BHC NA ALPHA-CHLORDENE /2 NA ENDOSULFAN T (ALP~A) O,K BETA LMLUN.lJl:Nt /"/_ W\ DIELDRIN NA GAMMA-CHLQRDENE /2 NA 4,a·-[lOl 1• P. P' -DDT~ NA. I -H-YTJRU,; Y• .. HLL1tWt'Nt /2 NA 4. 4' -DDE (P.P'-DDEl W', GAMMA-CHLORD!,IJE /2 NA '1,4'-DDD (P,P'-DDD) NA I WllM'::--!l!f_l!',JAf_"HLOR /0
O,M LNDRiN NA ALPHA-CHLORnANF /2 N.~ ~NOOSULF Af-J I I (BETA) NA ·cJS-NONACHLOR /2 NA FNOOSl.lLF.ti.N SIJLfATE NA (JX V(,Ht _1Wl}AN!::: ( on ACHLOREPOX IDE) /2 ~JA CHLORDAf-JE (TECH. r,iJXTUREl /1 NA METHOXYCI !LOR 5(1(lU PCB-1242 CAROCLOR 1242) NA FNll~lN ~EWNE 500U PCB-;254 <AROCLOR 12$4 J 15 PERCEiJT MOISTURE soou PCB-1221 (AROCLO~ 1221)
•••FOOTNOTFS.s••
-tA-·A'JEr.AG[ v:.LU[ •1-JA-NOT ANAL'v"/FD .,..,,lll-l"-l!ERFERHJCES •J-ESTH.~,'\TED VALUE •~-J-PR[SUMPTiVE EVIDENCE OF PRESENct: Of-MATERIAL
•~.-ACTUAL VALUE IS KtJOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAI VALIIE JS KNOWN TO BE GREATER THAtJ VALUE GIVEN
•LI-MATERIAL WAS ANAL Y?EO F<J~ ~IJT NOT DETECTED. THE NUMBER IS TIIE MHJ:MUM QUAIJTITATION LIMIT. C-CONFJRMED BY GC/MS
1. WHEN NO VALUE IS REPORT[D, SEE CHLORDANE CONSTITUFNTS 2. CONSTITUENTS OR METABOLITES OF TECHIJICAL CHLORDANE.
-
--·-- - - -- - - - -
PEST!CIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD. ATHENS. GA. ..
•• •• ..
................................ ****
PROJECT NO. 90-785 SAMPLE NO. 48883 SAMPLE TYPE: SOIL SOURCE: CAROL I NA TRA.NSFORMER STATION ID: 16-SLA
' . ' PROG ELEM: SSF CITY: FAYETTEVIL COLLECTION START:
--
COLLECTED BY: D THOMAN
ST: NC
--
08/07/90 0825 STOP: 00/00/00
-09/19/90
••• ' ••• '* * •••• *. * • * * •• * •••••• * * *. * * * * •• * • * •••• * * •••••• * * •••••••••••• UG/KG AIJAL YT I CAL RE SUL TS l/G/~.G ANALYTICAL RE SUL TS
NA ALDRIN 560DU PCB-1232 ( AROCLOR 1232) NA HEPTACHLOR 5600U PCB-1248 (AROCLOR 1248) NA HEPTACHLOR EPOXIDE 46000 PCB-1260 ( AROCLOR 1260) tJA ALPHA-BHC 5600U PCB-1016 (AROCLOR 1016) NA BETA-BHC NA TOXAPHENE NA GAMMA-BHC (LINDANE) NA CHLORDENE /2 NA DELTA-BHC NA ALPHA-CHLORDENE /2 NA ENDOSULFAN I (ALPHA) NA BET A CHLOROENE /2 tJA D!ELDRJN NA GAMMA-CHLORDENE /2 NA 4,4'-00T (P.P'-OOTJ NA 1-H'<Uf<OXYCHLOROE>ff /2 NA 4.4'-DOE (P.P'-DOEl tJA GAMMA··CHLOROAIJE /2 NA 4,4'-00D lP.P'-DDDJ NA TRANS-NONACHLOR /2 NA [NORIN NA ALPHA-CHLOROANF /2 tJA ENDOSULFAN II (BETA) NA CIS-NONACHLOR /2 NA ENDOSULFAN SULFATE NA OXYCHLOROANE l OCTACHLOREPOX IDE) /2 NA CHLORDANE (TECH. Ml XTURE l /1 NA METHOXYCHLOR 5600U PCB-1242 (AROCLOR 1242) NA FNOR!N KETONE 45000U PCB-1254 (AROCLOR 1254) 23 PERCENT MOISTURE 5600U PCB-1221 ( AROCLOR 1221)
••*REMARKS~*•
•••FOOTNOTES•••
•A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN •LI-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE M!IJlMUM QUANTITATION LIMIT. C-CONFIRMED BY GC/MS 1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-
-·-· -- - - -
PESTICIDES/PCB'S DATA REPORT
- - - --SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD. ATHENS, GA.
• • • • • • • • • • • • • • * • • • • • • • • • • • • • * • • • • PROJECT NO. 90-785 SAMPLE NO. 48884 SAMPLE TYPE: SOIL SOURCE: CAROLINA TRANSFORMER
-- -
BY: D THOMAN
ST: NC
-... .. .. .. .. STATION ID: 16-SLB
PROG ELEM: SSF COLLECTED CITY: FAYETTEVIL COLLECTION START: 08/07/90 0835 STOP: 00/00/00
UG/KG ANALYTICAL RESULTS IJG/KG ANALYTICAL RESULTS
NA ALDRIN 120U PCB-1232 (AROCLOR 1232) NA HEPTACHLOR 120U PCB-1248 (AROCLOR 1248) NA HEPTACHLOR EPOXIOE 110J PCB-1260 (AROCLOR 1260) NA ALPH/1-BHC 120U PCB-1016 (AROCLOR 1016) NA BETA-BHC NA TOXAPHENE NA GAMMA-BHC (LINDANEJ NA CHLORDENE /2 NA DELTA-BHC NA Al. PH.A-CHLORDENE /2 NA ENDOSULFAN I (ALPHA) NA BETA CHLORDENE /2 NA DIELDRIN NA GAMMA-CHLORDENE /2 NA 4.4'-DDT (P.P'-DDT) NA 1 -HYDROXVCHLORDfNf /2 NA 4.4'-DDE (P.P'-DDEl NA GAMMA--Cl ILORDAf~[ /2 NA 4,4'-DDD (P,P'-DDDJ NA TRANS-NONACHLOR /2 NA [NORIN NA ALPHA-CHLOROANF /2 tJA EtJDOSULF AIJ I I (BETA) NA CIS-NONACHLOR /2 NA ENDOSULFAN SULFATE NA OXYCHLORDANE (OCTACHLOREPOXIDE) /2 NA CHLORDANE (TECH. MIXTURE) /1 NA METHOXYCHLOR 120U PCB-1242 (AROCLOR 1242) NA FNOR!N KETONE 100U PCB-1254 (AROCLOR 12541 12 PERCENT MOISTURE 120U PCB-1221 CAROCLOR 1221)
--09/19/90
• • • ... ..
•• .. ..
•••FOOTNOTES••• •A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-EST!MATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS ~.NOW~J TO BE GREATER THAN VALUE GIVEN •LI-MATERIAL WAS ANALYZED FOR ~UT NOT DETECTED. THE NUMBER IS THE MIIHMUM QUANTITATION LIMIT. C-CONF !RMED BY GC/MS 1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
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--·---- -- - - --- -- ---SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION JV ESD. ATHENS. GA. PESTICIDES/PCB'S DATA REPORT ... ..
•• • • • •
• .. • • • • • • • • • • • * * • * • • • • • • • * * * • * *
PROJECT NO. 90-785 SAMPLE NO. 48897 SAMPLE TYPE: SOIL SOURCE: CAROLINA TRANSFORMER STATION ID: 17-SLA
• • • .f. • • • .. • • * • • • • • • • • • * • *
PROG ELEM: SSF CITY: FAYETTEVIL COLLECTION START:
COLLECTED BY: D THOMAN ST: NC 08/07/90 1010 STOP: 00/00/00
09/19/90
• • • ••• •• .. •• •• ♦♦♦ ♦ ♦ ♦ ......... *. *. * ••• * ••• * * * * * • * * • * * * * •• * * ••• * ••••• * • * •••• * •• * * * * *** UG/KG ANAL YT! CAL RESULTS IJG/KG ANALYTICAL RESULTS
NA ALDRIN 4500U PCB-1232 (AROCLOR 1232) NA HEPTACHLOR 4500U PCB-1248 (AROCLOR 1248) NA HEPTACHLOR EPOXIDE 94000 PCB-1260 ( AROCLOR 1260)
NA ALPHA-BHC 4500U PCB-1016 (AROCLOR 1016)
NA BETA-BHC NA TOXAPHENE NA GAMMA-BHC (LINDANEl NA CHLORDENE /2 NA DELTA-BHC NA ALPHA-CHLORDENE /2 NA ENDOSULFAN I (ALPHA) NA BETA CHLOROENE /2 NA DIELDRIN NA GAMMA-CHLORDENE /2 NA 4,4'-DDT (D,P'-DDT) NA 1-HYDROXYCHLORDENE /2 tJA 4,4'-DDE CP.P'-DDE) NA GAMMA .. CHLORDAIJ[ /2 NA 4,4'-DDD (P,P'-DDD) NA TRANS-NONACHLOR /2 NA ENDRIN NA ALPHA-CHLORnANE /2 tJA ENDOSULFAN II (BETA) NA CJS-NONACHLOR /2 NA ENDOSIJLFAN SULFATE NA OXYCHLORDANE (OCTACHLOREPOXIDE) /2 NA CHLORDAIJE ( TECH. MIXTURE) /1 NA METHOXYCHLOR 4500U PCB-1242 (AROCLOR 1242) NA ENnRIN KETONE
90000U PCB-1254 (AROCLOR 1254) 21 PERCENT MOISTURE 4500U PCB-1221 ( AROCLOR 1221 )
•••FOOTNOTES••• •A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPTJVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE JS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM OUANTITATION LIMIT. C-CONF!RMED BY GC/MS 1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
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--- - - - -- - - - -
SAMPLE AIID ANAL VS! S MANAGEMENT SY5 TEM
EPA-REGION IV ESD, ATHENS, GA.
- - - - -
PtST JC!OtS/PCB'S DATA REPORT ... .. .. .. ••
•••••" ... • .. ••••••••""**••TT,-~T1'
PROJECT NO. 90·-785 SAMPLE NO. 48898 SAMPLE TYPE: SOIL
SOURU: r.AROL I NA TRANSFORMER
STATION ID: 17-SLB
• • • • • • • ♦ • • • • • • • • • • • • • • • • • • • •
PROG ELEM: SSF COLLECTED
CITY: fAYETTEVIL
COLLECTict~ START: 08/07/90
BY: D THOMAN
ST: NC
1020 STOP: 00/00/00
-
09/22/90 ... •• •• ..
• • ••• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • * .................................. .
UC/KG Ah/AL VT I CAL RESULTS 1.IG/!".G At:AL \'T!Ct.L ~['.:iLlL TS
tJA NA NA
~!/\
NA
NA
'1A
NA
NA NA
NA
NA
l'IIM.. HA
NA
tJA 6bOU
20000U
560U
ALDRHJ
HtPfACHLOR
HEPTACHLOR EPUX!Ot .'\Lf-'H.~,. BHC
BU A-BHC
GAMMA-BHC (LINDANEJ
OEL T ti.-BHC
ENDOSULFAN I (ALPHA)
CJELDRIN a a•-nnr Ip o•-nnr)
4:4'-DDE iP:P'-DDEl
4.4'-DDD (P,P'-DDD) [NURIN
EtJD05ULf AN I I (BETA)
l:J\IOQSULFAN SIJLf/\TE
CHLORDANE (TECH. MltTUREI /1
PCS-1242 (AROCLOR 1242)
PCB-1254 ( AROCLOR 1 ?54)
PCB-1 ~21 ( AROCLO~ 1221}
•••FOOTNOTES•••
660U
660U
22000
660U
NA
NA NA
1JA NA
Ni.I.
N~ NA NA NA NA
UI'.
NA
19
PCB-1232 (AROCLOR 1232)
PC!;-12,,8 ( .'\RIJCLOR 1248) PCB-1260 i AROCI. OR 12601
PCB-1016 (AROCLOR 101G)
TOXAPHENE
CHLORDENE /2 ALPHA-CHLURDENE /2
SETA CHLORDFNf. ;2 GMIMA-CHLORDENE / 2
l-rlff1kt)Xv1 .. +;Ll_•f<OfNf /2
GAMMA-CHLORD,'\NE /2
1 WAl\1'::,-M(lf'!.O.f:HLOR ,' 2
ALPHA-CHLOROANF /2
CIS-NONACHLOR /2
CJXYCHU)ROANt (Clf:Tt!i<::HLIJREPOXIDE) /2
METHCX'/CflLOR
fNllk!N KEfONE
PERCENT MOiSTURE
,-A-AVE~AGE VALUE •hiA-NOT ANAL"Y7f.D •NAJ-!Mlt:Rft:P.ENCES "'J-ESTIMATED VALUE •rJ-PRESUMPIIVE EVjDENCE OF PRF.SENCt Ut-MATERIAL
•K-ACTIJAL VALUE IS KNOWN TO BE LESS THAfJ VALUE GiVEN •L-ACTUAI. VALUE 15 KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALV7F:n F(J~ 1:HII MOT DETECTED. THE UUMBER IS THE MHHMUM QUANT:iTATION LIMIT. (-CONFIRMED BY GC/MS
1. WHHJ NO VALUE IS REPORT[D, SEE CHLORDANE CONSTITUFNTS 2. CONSTITIJEfJTS OR METABOLITES OF TECHNICAL CHLORDANE.
-
-- --- ---- - - - - - --
PESIICIDES/PCB'S DATA REPORT ... .. .. .. ••
......................
PROJECT NO. 90-785 SAMPLE SOURCE: CAROLINA TRANSFORMER STATION ID: 18-SLA
* • • • •
NO. 48895
UG/KG ANALYTICAL RESULTS
NA ALDRIN NA HEPTACHLOR NA HEPTACHLOR EPOXIDE NA ALPHA-BHC
NA BETA-BHC NA GAMMA-BHC (LINDANE) NA DELTA-BHC NA ENDOSULFAN I (ALPHA) NA DIELDRIN
NA 4,4'-0DT (P,P'-DDT)
NA 4,4'-DDE (P,P'-DDE)
NA 4,4'-DDD (P,P'-000) NA [NORIN
NA rnoo~ULFAN II (BETA)
NA ENDOSULFAN SULFATE
NA CHLORDANE (TECH. MIXTURE) /1 5800U PCB-1242 (AROCLOR 1242)
50000U PCB-1254 (AROCLOR 1254) 5800U PCB-1221 ( AROCLOR 1 221 )
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.
• • • • • * • • * * • • • * • • • ' • • •
SAMPLE TYPE: SOIL
• • • • • * • • • • • *
PROG ELEM: SSF CITY: FAYETTEVIL
COLLECTION START:
COLLECTED BY: D THOMAN ST: NC
08/07/90 0950 STOP: 00/00/00
ANALYTICAL RESULTS
5800U PCB-1232 (AROCLOR 1232) 5800U PCB-1248 (AROCLOR 1248)
100000 PCB-1260 (AROCLOR 1260)
5800U PCB-1016 (AROCLOR 1016) NA TOXAPHENE NA CHLORDENE /2 NA ALPHA-CHLORDENE /2 NA BETA CHLORDENE /2 NA GAMMA-CHLORDENE /2 NA 1-HVOROXYCHLORDfNI' /2
NA CAMMA-·CI ILORDAIJE /2 NA TRANS-NONACHLOR /2
NA ALPHA-CHLOROANI' /2 NA CIS-NONACHLOR /2 NA OXYCHLORDANE (OCTACHLOREPOXIDE) /2 NA METHOXYCHLOR NA fNOR!N KETONE 27 PERCENT MOISTURE
••*REMARKS*•*
-09/19/90 ... .. .. ..
••
•••FOOTNOTES*** •A-AVERAGE VALUE •NA-cNOT ANALYZED •NAI-INTERFERENCES •J-EST!MATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS r.NOWN TO BE GREATER THAN VALUE GIVEN •U-MATER!AL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER 15 THE MlNlMUM QUANTITATION LIMIT. C-CONflRMED BY GC/MS 1. WHnJ NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. COfJSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-
-·-- --- -
Pt~TICIOtS/PCB'S DATA REPORT
- ----SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EP.ll.-P.EGimJ IV ESD, ATHEr~s. CA.
- --
• • * * • • • • • • * • * • * * • * • • • • • * T T T ~ T * • • • ♦ • ♦ ♦ ♦ • * • • • • • • • • • • • • •
PROJECT NO. 90-785 SAMPLE NO. 48896 SAMPLE TYPE: SOIL PROG ELEM: SSF SOURC.F: CAROLINA TRANSFORMER COLLECTED BY: D THOMAN ST: NC
- -
... •• •• .. .. STATION ID: 18-SLB Cin': fAYETTEvIL
C0LLECTim~ START: 08/07/90 1000 STOP: 00/00/00
!JC/KG ANALYTICAL RESULTS
IJA ALDR HJ 660U PCB-1232 \AROCLOR 1232) NA HtP rnCHLOR 660U PCtl-12:'18 (AROCLOR 1248) hiA HEPTACHLOR EPOX!DE 8600 PCB-1260 ( AnOr.tOR 1?'30) ~Y\ :\:..P:·:A EH!C 660U PCB-1016 ( AROCLOR 1016) NA BEIA-BHC NA TOXAPHENE NA GAMMA-BHC ( LINDANE l NA CHLORDENE /2 MA DEL T.b.-BHC NA AlYHA-CHLOROENE /2 NA ENDOSULFAN 1 (ALPHA) ,-H SETA L.nLUtl.Ur:Nc /2
NI\ DIELCRHJ MA G/1.MMA-CHLORDENE /2 NA 4,4'-lll_)'I (P.P'-C'DT) IJA l -HY Ut<(Jx. Y(-HLU~!)t: NF.. /2 IJA 4,4'-DDE (P.P'-DDEl ~/\ GAMr.~A-CHLORDl\i~E /2 NA 4,4'-DDD (P,P'-DDD) NA TW "-"l':::--M(l!',!_!l_(!-!L OR •?
i-iA [NUr\lN tJA ALPHA-CHLOROANf' /2 fJA ENDOSUL f AIJ l 1 (BEiA) NA CIS-NONP.CHLOR /2 NA FN0051.IL f .AN SULf/\fE NA OXYCHL(IKDAN!:: ( Or'TACHLOR!:POX I DE) /2 NA CHLOROt.lJE (TECH. MIXTURE) /1 NA METHOXYCI ILOR 61:'iOll PCB-1242 (AROCLOR 1242) NA eNllR!N ,.ET ONE
8500U PCB-1254 ( ARt)CLOR 1254) a~ P[RC[NT MOlSTURE LO 550U PCB-1221 (AROCLCR 122i)
•••FOOTNOTf5•••
-
U\J/22/90
"' .. .. ..
TA-AVERAGE 'v'ALUE +l~A-NOT ANAL\i/Ef) •MAf-1111•tH~ERENCES •J-ESTIMATED VALUE :s;J-PR[SUMPTIVE EVIDENCE Of ~RF.SENCI: UI-MATERIAL •K-ACTLIAL VALLIE IS KNO\'ltJ TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS ,.NOWN TO BE GREATER THAN VALUE GIVEN
•LI-MATERIAL WAS ANALY::?f:O Fr_lw ~IJT t-JOT DETECTED. THE ~JU~.,SER IS THE MHJIMUM QUAfJTITATiON LIMIT C-CONF!RMEO 8V GC/MS
1. WHEN NO VALUE IS REPCRTCD. S[E CHLORDANE CONST!TufNb 2. COMST!T 1.'ENTS OR METABOLITES OF TECHIHCAL CHLORDANE.
-
--·-- ---- -- - - - ---- -
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION JV ESD, ATHENS, GA. ... ................................ "**••••:r• PROJECT NO. 90-785 SAMPLE NO. 48893 SAMPLE TYPE: SOIL SOURCE: CAROLINA TRANSFORMER
• • *
BY: D THOMAN ST: NC
.. .. .. .. STATION ID: 19-SLA
PROG ELEM: SSF COLLECTED CITY: FAYETTEVIL COLLECTION START: 08/07/90 0935 STOP: 00/00/00
UG/KG ANALYTICAL RESULTS ANAL YTJCAL RESULTS
NA ALDRIN 5100U PCB-1232 (AROCLOR 1232) NA HEPTACHLOR 5100U PCB-1248 (AROCLOR 1248) NA HEPTACHLOR EPOX JOE 550000 PCB-1260 (AROCLOR 1260) NA ALPHA-BHC 5100U PCB-1016 (AROCLOR 1016) NA BETA-BHC NA TOXAPHENE NA GAMMA-BHC (LINDANE) NA CHLORDENE /2 NA DELTA-BHC NA ALPHA-CHLOROENE /2 NA ENDOSULFAN I (ALPHA) NA BETA CHLORDENE /2 NA DIELDRJN NA GAMMA-CHLORDENE /2 NA 4,4'-DDT (P.P'-DDT) NA 1-HYDROXYCHLDRDENI' /2 tJA 4,4'-DDE (P,P'-DDEl NA GAMMA··CHLORDAtJ[ /2 NA 4,4'-DDD (P,P'-DDD) NA TRAN~-NONACHLOR /2 NA ENDRIN NA ALPHA-CHLOROANI' /2 NA EtJDOSULFAN II (BETA) NA CIS-NONACHLOR /2 NA ENDDSULF~.N SULFATE NA OXYCHLORDANE (OCTACHLOREPOXIDE) /2 NA CHLORDAtJE (TECH. Ml XTURE) /1 NA METHOXYCHLOR 5100U PCB-1242 (AROCLOR 1242) NA FNDRIN KEIONE sooooou PCB-1254 (AROCLOR 1254) 27 PERCENT MOISTURE 5100U PCB-1221 ( AROCLOR 1221 l
•"•REMARKSu•
•••FOOTNOTES*••
09/19/90
• • • ... .. .. ..
••
•A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-ESTJMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE JS KNOWN TO BE LESS THAtJ VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN •U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE M!tJIMUM QUANTITATJON LIMIT. C-CONFJRMED BY GC/MS 1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-
---- -
PESTJCIUES/PCB'S DATA REPORT
NO. 48894
liiiil liiiii liiii iiiii -- - -
SAMPLE AND ANALYSIS MANAGEMENT svqEo,,
EP.6.-REGION !'./ ESD, ATHE~JS, CA.
SAMPLE TYPE: SOIL PROG ELEM: SSF COLLECTED CITY: ,AYtTTEV!L BY: D THOMAN ST: NC
--
..
•• .. ..
PROJECT NO. 90-785 SAMPLE SOU RU: (AROL I NA TRM!SFDP.MER STATION ID: 19-SLB C0U .. ESTim~ ST:.RT: 08/07/90 0940 STOP: 00/00/00
♦ .. .. ♦ +. • ~ ♦ ... • • • " • • • * * • • 11 • • • • • " ,. " .t" :J " " " .-t; l-♦ " ... * • "' • • • UC/KG ANALYTICAL RESULTS 0G/~G
NA ALDRIN 6501J N.A HEPIACHLOR 13601) NA HEPTACrlLOR EPOXJDE 36000 ~!II. A!..l"llA· e11c 660U NA BEIA-BHC NA
NA GAMMA-BHC ( L!NDANE l NA NA DELTA-BHC NA NA ENDOSULFAN l (ALPHA) "H ~!A D!ELDRIN MA NA 4,4'-P!J'f 1. P. P' -!)DT) NA NA 4.4'-DDE (P.P'-DDEl NA NA 4.4'-DDO (P,P'-DDDJ NA "H [NURIN NA
~M EN8CISLJLF AfJ I I (BETA J NA NA FNnlJ5llLFAN SUL f :'\TE NA
tJA CHLOROAIJE (l[CH. MiXTURE) II ~!A 6bOU PC8-1242 ( AROCLOR 1242) NA 35000U PCB-1254 ( AROCLOR 1 :?.54) 2:l 650V PCB-1221 ( AROCLOR 1221)
At~A!... '.'TI CAL
PC:3-1232 ( AROCLOR 'i 232 l
PCl3-12/48 ( /IROCLOR 1248)
PCB-1260 (AROf.LOR 1260) PCB-1016 (AROCLOR 1016) TOXAPHENE
CHLORDENE /2 ALPHA-CHLORDENE /2
DC I'"' \.,t1LUKUr.Nr. i L G/\MMA-CHLOROEtJE /2 1-H·v [1t<Ux Yt_.t-H_OR:Ln-:t-Jf /2 GA~,1MA-CHLGRDAhlE /2 lk AMS-!'!•.1!'-J.6.r.:HL O?. /2 ALFHA-CHLORnANF /2 CI 5-tJONIICHLOR /2
,-.,-, '" -rr l\l--'..lVL I.:,
(J)( VI.HI. c"!R(Jllf\lE ( or r a.r.~L ORE POX I DE)
r.~ETHOX'.'CI :LOR fNIJR IN KtfONE FCRCENT t.iOISTURE
/2
-Oll/22/90
•• •• •• . . ...
•••FOOTNOTEC.•••
-rA-AVE~:.G:: VALUE •hiA-hiOT ANAL",(7fD •Mlll-HJIERFERENCES •J-ESTlMATED·VALUE itJ-PRLSUr...t~TIVE EViDENCE OF PRESENCE 0~ MATERIAL •K-ACTU~.L VALVE IS KNOWtJ TO BE LESS THAN VALUE GIVEN •L-ACTUAl VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•LI-MATERIAL WAS ANALY7.f0 Fr.1~ !:\LIT NOT DETECTED. THE NU!.~SER IS THE MINIMUM OUANTITATION LIMIT. C-CQNFIRMEO 9V GC/MS
1 . WHEH t~O VALUE IS REPORTED. Si:E CHLORDANE CONST I TUF NTS. 2. COMST I TL'E~JTS OR METABOLITES Of T[CHIH CAL CHLORDANE.
-
I'
[
.~l
---- ----- ----- -- - --
PtSfJCJDtS/PCB'S DATA REPORT ... ..
•• .. ..
• ♦ • • • • • • • • • • • * •
PROJECT NO. 90-785 SAMPLE SOURGF: CAROLIN~. TRANSFORMER STATION ID: 20-SLA
. . --. NO. 46881
SAMPLE AND ANALYSIS MANAGEMENT ~YSTcM
EPA-REGION IV ESD, ATHE.t~S. GA.
• ♦ * ♦ T T ~ T ~ ♦
SAMPLE TYPE: SOJL • • • PROG ELEM: SSF COLLECTED CITY: FAYUTEV!L COLLECTION START: 00/07/90
BY: D THOMAN
ST: NC 0825 STOP: 00/00/00
09/£2/90
' ' '
♦♦♦ ♦ ♦ ♦ I ♦ • ♦ ♦ ♦ ♦ ♦ ♦ ♦ * ♦ ♦ ♦ ♦ ♦ ♦ * ♦ T * ♦ T ♦ ♦ ♦ ♦ ♦ ♦ ♦ • • ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ~TT• T ♦ T ♦ T
UC/Y.G AIJALYTICAL RE SUL TS IJG/!-1'.G MJ.!.L \'TICA:.._ ~;:::.uL r:;
NA ALDRII, 950IJ PCB-1232 (/.ROCLOR i232) t,JA HtP lft.CHLOR 950U PCB-12/\8 ! /\ROCLOR 1~48) NA HEPTACHLOR EPOX !De 14000 PCB-1260 ( AROCI OR 1 ?00 l
H:'\ ~:...rHA-e1 :c 950U PCB-1016 ( AROCLOR 1016) NA Bt!A-BHC NA TOXAPHENE NA GAMMA-BHC ( L!NDANE) NA CHLORDENE /2 NA DEL T.b..-BHC NA ALPHA-CHLl'RDEME /2 NA ENDOSULFAN I ( ALPHA) "~ 6ETA Ci-ii..URUF:NE IL NA D!ELDRIN NA GAMMA-CHLORDENE /2 NA 4,a'-l)fH 1.P.P'-DDT) NA 1-1-1YiJKOX:v(.HLIJf<!JtNf /2 tJA 4,4'-DDE (P.P'-DDEJ ~~A GA~:.M:..--CHLORU/1iJE /2 'IA 4.4'-DDD ( P. P' -·DDDJ "'" 1 WllM':::,-Ml_lM_6_r_:HL0R M
iJA [NC,riiN IJA ALPHA-CHLOROANF /2 tJ.i\ EtJDOSULf :..:J l I (BETA) NA CIS-NONACHLOR /2 NA Ft-iDOSIJLFt>N SIJLf/\TE NA l-l X Y(:HI _ l)f<l)At-.!I: ( OCT ACHLOP.EPOX IDE) /2 tJA CHLORDAtJE (T[Cfi. MIX.URE) /1 tJA ME THCXYCI ILCR
9~•,f)lJ PCB-1242 (AROCLOR 1242) NA fN!lR]N KETONE 10000U PCB-1 ?54 ( AROC.LClR l JCi4 _) 15 PERCEi<T lviOI STliRE 950U Pce-1221 (;..ROCLCR 1221)
•••FOOTNOTES•••
T A-A'..'ERAGE \,'/..LUE •i.JA-NOT ANAl.·v·7FO a NA I-1 MI ERFERENCES • J-ES T U.~ATED VALUE 1-:J-PRLSUMPI 1 VE EV j DENCE OF F'RESENCi:: UF MO.TER IAL •r.-ACTUAL VALUE IS KtJOWN TO BE LESS THAIJ VALUE GIVEN •L-ACTUAL VALUE IS r.NOW!I/ TO BE GREATER THAN VALUE GIVEIJ •LI-MATERIAL WAS ANALY2FO FUH BUT NOT DETECTED. THE NUMBER IS TIIE MINIMUM QUANTITATION LIMIT. C-CONF!RMED BY GC/MS
1. WHEN ~m VALUE IS REPORi[D. SEE CHLORDANE CONSTITUFNT$_ 2. CONSTITVnns OR METAeOLlTES OF TECHIJICAL CHLORDANE.
-
---- - - - - - ------ --- -
~ESIICIUtS/PCB'S DATA REPORT
SAMPLE AND AIJALYSIS MANAGEMENT SV5TE"'
EP.A.-REGION IV ESD, ATHE~~S. GA.
♦ ♦ f ♦ f f * f f f f f f * * * f * * * * * f f T T T ~ ~ ~ * • • PROJECT NO. 90-785 SAMPLE NO. 48882 SAMPLE TYPE: SOIL
SOURCE: CAROL I Nh. TRA.NSFORt.lEP. PROG ELEM: SSF COLLECTED BY: D THOMAN
ST: NC
... .. •• .. .. STATION ID: 20-SLB CITY: FAYtTTEV!L
COLLECTIO:J STArn. OG/07/90 0830 STOP: 00/00/00
UC/Y-.G Al.JAL 'IT I CAL RE SUL TS
IJA ALDRIN 65:JU F'CS--'l 232 {AROCLOR 1232) NA HEPTACHLOR 6601) PC~-12'l9 !AP.OCLOR 12.!!8) NA HC?TACHLOR EPOXIUE 4700 PCB-1260 ( AROU OR 1?60) ~!.'\ /\Lt':-iA··Cl:C 660U PCB-1016 (AROCLOR 1016) NA BtTA-BHC NA TOXAPHENE NA GAMMA-BHC ( LI NDANE) NA CHLORDENE /2 MA DELTA-BHC NA AIYHA-CHLORDENE /2 NA ENDOSULFAN 1 (ALPHA) O,M 6ETA l.MLUKurNt /2 W\ D!ELDRIN MA GAMM/\-CHLORDENE /2 NA " ,4'-DUT '.P.P'-!:'DT) NA i -1-fri:J1<(JXYCHLUKD!:Nt /2 NA 4,4'-DDE (P.P'-DDEl W\ GAMMA-CHi...CrW~\iJE /2 '" .d 4 1 -nnn ( P, P' ·-DDD) NA rw OM':::--M'.lM_.o.<;H!...QR /2 ;~A i:i~URlN--IJA ALPHA-CHLORDANF /2 ~J/1. e~CCSULF A~J I I (BETA) NA CIS-NONACHLOR /2 NA l:NDOSIJLFti.N SLIL!-'/\1E NA CJ>(v(.HI Ol'.:.1:t.lA"'JI: l 0 1.~T ACHLOREPOX IDE) /2 t~A CHLORD1\i-JE (T[CH. MJ,TUREl _/ 1 NA METHOXYC: 1LOR 6ti< I'../ PCB-1242 (AROCLOR 1242) NA fNllRJN KE I ONE 4500U PCB-1254 ( AROCLOR 12'i41 1 .; PCRC[i~T MGISTURE 560V PCB-1221 {AROCLOR 1221 )
• • • FOOTNOTF.S• • •
O!J/22/90
T T > .. ' .. ..
• • . .
TA-AVEr..t.G[ VALUE •hiA-NOT ANALY7f:TJ •NA!-JNIERFEP.HKES •J-ESTIMATEO VAL:JE ,rJ-PR(SUiviPTIVE EViDENCE OF ~RE5£Nct ut· MATERIAL
•~.-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAt. VALUE IS KNOWN TO BE GP.EATER THAN VALUE GIVEN
•U-MATERIAL WAS ANAI.Ylfn FI.\R ~llT NOT DETECTED. THE tJUMBER IS THE MHJH,:UM QUANTJTATION LIMIT. C-CONFJRMED BY GC/MS
1. WHEiJ IJO VALUE IS RffORTCD, SEE CHLORDANE CONSTITUFNT'-2. CONSTITUENTS OR METABOLITES OF TECHIJICAL CHLORDANE.
-
-·-- --- -
PtSJICIUtS/PCB'S DATA REPORT
NO. 48879
- ----SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EP.t..-P.EG!ON !~1 ESD, ATHE~JS, GA. - --
BY: D THOMAN
ST: NC
- -
..
•• .. ..
PROJECT NO. 90-785 SAMPLE SOURC:f: CAROL! Ml\ TRAMSFOP.MER STAT!Of, ID: 21-SLA
PROG ELEM: SSF COLLECTED CITY: fAYtTTEVIL
C0LLECTIOtJ STA~T. 08/07/90 0800 STOP; (nl/00/00
~+• + f ♦ • f + • • • • • • * • • * * * • * * * * * T T * * * * * * * • + ♦ • • f • • * UC/KG A.IJ/..,LVTICAL RESULTS •.'G.'Y.G
fJA NII
l,A
~!.'\ NA NA NA f,A
~lJ\ NA fJA .,,
i,JA N,'\ NA
tJA
6tif )II
1 sooou 6SOU
ALDRHJ HEPIACHLOR HEPTACrlLOK EPOX!Oc "'t ('\llfl .• D• If" Bt,A~BHC'"' GAMMA-BHC ( LI NDANE l
DEL T.l~.-BHC
ENDOSULFAN l ( ALVHA)
DIELC~HJ
.d 4' -rnn Ip D 1 -nnT \
4:4'-DDE iP:P'-DDE) A,4'-DDD (P,P'·-DDD)
Cr.il/iHN ENDCSULFAN II (BETA)
F.NOOSJJLFM! SIJLf/\TE CHLGRDHNE (T[CH. MIATUREi /1
P(B-1242 ( .1'1.RQCLOR 1242)
PCB-1254 ( AROCLOR 1 ?54 .1 Pee-, 221 ( AR0CL0R 1221}
•••FOOTNOTES•••
560tl
6t>OIJ 17000
6601J NA NA NA ,.M
~J.I\ NA
tJA NA
NA NA
liA Nf-, NA
7.--1
F'CB-1232 ( ,\R0CL0R 1232)
PCB-1 2'18 ( .l\ROCLCR 1248) PCB-1260 r AROCI. OR 1 ?iSO l PCB-1016 (AROCLOR 1016) TOXAPHENE CHLORDENE /2
ALSHA-CHLORDENE /2
ot. 1 f'I L,MLUKUr: Ne /2
Gt-,MM/\-CHLORDEUE /2 ~ -:-::v~·:,K~:~vc_;~L\l~;~t"Nt-, /2 uAmm,...--....,nLOr,DHNt. / 2
I W.0.N';,-!'-!f_l!',]_6_f_"HLOR /2
ALPHA-CHLOROANF /2 CJS-NONACHLOR /2
O>Cv'CHl.fJRLlANC (OCTA(HLQR.EPOXIDE) /2
METHOXYCI !LOR
f:'NORIN KETONE
PERCENT MOISTURE
• -1-,. REMARKS••"
-OYn2/90
•• •• • • .. ...
TA-AVERAGE './AU.IE •I-.IA-NOT ANAL"v'/fr, •MA1-1NIEP.fE~HJCES •J-EST!MATEC VALUE :s:N-F'R[S;JMPTIVE EVIDENCE OF ~Rf.SENCt Ut-M.O.TERIAL •K-ACTLl•.L VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAI. VALIIE IS KNOWN 10 BE GREATER THAN VALUE GIVEIJ •LI-MATERIAL WAS ANAI.YZFn FOH ~IJT NOT DETECTED. THE NU~BER IS Tl:E MINIMUM QUANTITATION LIMIT. C-CONF!RMED 9Y GC/MS
1. WHEU ~W VALUE I~ R[F'ORTCD. SEE CHLORDANE CONSTITUFNT'S. 2. COMSTITL'ENTS OR METABOLITES OF TECHtJICAL CHLORDANE.
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PfSfJCIUtS/PCB'S DATA REPORT ... .. ••
" ..
. . . . . . . . . . . . . . ..
PROJECT NO. 90-785 SAMPLE SOUR CF: CAROL I NA TP.M!Sf'ORMER STATION ID: 21-SLB
.. . . .. .
rvo. 4Bsso
-------- --SAMPLE Al,D ANALYSIS MANAGEMENT SYSTEM EP.~.-REGION IV ESD, ATHnJS, GA.
.. .. .. .. • t ~ ~ ~ *
SAMPLE TYPE: SOIL PROG ELEM: SSF COLLECTED CITY: f'AYtTTEVIL
COLLECTirnJ START. 08/07/90
BY: D THOMAN
ST: NC
0810 STOP: 00/00/00
-
0~/22/90
". .. .. .. .. ~♦~ ♦ ♦ • ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦• * .... ♦ ♦ .... ♦ ♦ ♦ ♦ ♦ + ♦ ~ ~ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ •• T ♦ ♦ ♦ t ♦tt UC/Y,G AIJAL'i'TIC~L RESULTS •.'G/!<.G ~~JALVTICAL ~[JUL.TJ t,A hLDRlN 660U PCS-1232 ( ,\ROCLOR 1232) MA HEPfACHLOR 6601J PC~-121!8 ( !'.R:OCLCR 124e) NA HEPTACHLOR EPOX!Dt 4300 PCB-1260 ( AROr.lnR l?GOl ~!:\ t.1 f'HIII 811C 660U PCB-1016 (AROCLOR 1016) ...... , "" NA BtlA-BHC NA TOXAPHENE NA GAMMA-BHC ( L!NDANE J NA CHLORDWE /2 MA DELTA-BHC NA ALPHA-CHLORDENE /2 NA rnDOSULFAN I ( A1_'1HA) ... BETA L.MLUt'.Ut:l\ir: I 2. ,-M NA DIELDRIN N.A. GAM~J.A-CHLORDENE /2 NA 4. 4' -llf)f '-P. P' -DDT) NA 1-t·-iv"lJki'lX YtHLUKfJt"Nt: /2 rJA 4,4'-DDE (P.P"-OOE) .. , GA~.~r1~:..-~i~LORU1\i~E /2 .. ~ NA 11 .1•-nnn (P,P'-·DDD) NA I k'A/\1'::-,-Mf.l~!.6_<_·!,·H ... OR 10 i,iA t~tiRiN--NA ALPHA-CHLOROANF /2 ~JA EtJDC~:JLF AtJ l I (BETA) MA CIS-NONACHLOR /2 NA f.NOOSl.llf6_N SLILFl\fE NA (JXVt".HI. (ll<L)ANt ( or:T 0.CHLOREP0Y.I DE) /2 NA CHLOfWAi,i[ \T[CH. MIXTURE l /1 NA METHOXYCI ILOR 6tiflll PCB-1242 (AROCLOR 1242) NA fNllRIN K.E IONE 4000U PCB-1254 (ARO(L()R l;>S4l 11 P[RCENT MOISTURE 660U PC:8-1221 { A:-!OCLCR i 22i)
•••fOOTNOTfS•••
'tA--A\.'ERAG[ 'w'ALUE •NA-NOT ANAL"v'7f0 •"IAl-!M!E~fEREMCES •J-ESTIMATED VAL.t.:[ ,r..:-:>R[SUM?TIVE EViDENCE OF ~F<ESENCt: ur MA.TERlAL •K-ACTUAL VAL'JE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAI. VALUE IS K.NOWN TO BE GREATER THAN VALUE GIVEN •U-MATERIAL WAS ANAIYlFO F(l~ 81.IT flOT DETECTED. THE NUMBER IS TIIE MINIMUM QUAIHITATION LIMIT. C-CONF!RMED 9Y GC/MS 1. WHEII NO VALUE IS RE?ORT[O, SEE CHLORDANE CONSTITUFNT$. 2. COMST!Tl'ENTS OR METABOLITES OF TECHIHCAL CHLORDANE.
-
-- ---- -
~E51JCIOES/PCB'S DATA REPORT
- - - - -
SAMPLE AND ANALYSIS MANAGEMENT ~YSTEM
EP.1\-REG!O~J IV ESD, ATHEtJS, CA. ... ♦ • • ' • • • • * * * * * * * * * * * * * * * * * T * 'T ~ * * * * PROJECT NO. 90-785 SAMPLE NO. 48905 SAMPLE TYPE: SUIL SOURCF: CAROLIN~ TP.ANSFORMEP.
- --
BY: D THOMAN ST: NC
- -
..
•• .. .. STATION ID: 22-SLA
PROG ELEM: SSF COLLECTED CITV: fAYtTTEVIL
COLLECTimJ START: OG/07/90 11i5 STOP: 00/00/00
UC/KC AI.JALYTICAL RESULTS
NA ALGRJN NA HEPTACHLOR NA HEi'TACHLOR EPOX!OE ~1:'\ .".U'!lA··eHC NA BEIA-BHC NA GAMMA-BHC ( LINDANE) MA DEL U.-BHC NA ENDOSULFAN I (_ALPHA)
~!i\ DlELDRHJ NA "1_4'-0l_ll 1• P . P' -DDT J IJA 4.4' ·ODE <P.P·-00E1 NA 4,4'-DDD (P,P' -DOD) i..i:.. LNUR.iN NA E~~DOSULFAN ' . ( BEH,) " NA FMOOSl'LFAN SULf/\1E tJA CHLORDAiJE ( TLCH. MiXTUREl /1 9Sou PCB-1242 UROCLOR 1242) 25000U PCB-1254 i AROCLOR 1 ?54) 950U PCB-1~21 Z AROCLCR 1221)
•••FOOTNOTE,;•••
• • ~ * • ~ ~ • • • • • • ~ • • • • • • • • • • • • • • • • • • • Al1,\I "T'Tr-~, ,...,.,.,,, ..,.,. ,-;,•,nL.. 1 1 .1.\,,ML.. l,L..lUL I.:, HG/!<'.G
95CU PCS-1232 ( AROCLOR 1232) 9SOU PCB-12'18 ( l\ROCLOR 1248) 30000 PCB-1260 C AROCI OR 1 ?.fi() ) 950U PCB-1016 ( AROCLOR 1016) NA TOXAPHENE NA CHLORDENE /2 NA ALPHA-CHLORDENE /2 ,.M BETA CHLORDENE 12 NA GAl!MA-CHLORDENE -~ , L NA j -tfYOk'UX YI ,Hl(ll<Ut"Nt 12 NA GAr,~~.lA-CHL.ORDAi.JE I 2. NA l RA/\IS-f.J(l~J.<"_l:HLOP. M
tJA ALPHA-CHI.OROANF /2 NA CJS-NONACHLOR 12 NA OXY1-:H1_(lHLlANE <. (lr,r ACHLOREPOX IDE) /2 ~!A METHOX'.'CI ILOR NA fNIJSJN KEIONE J4 ?[RCENi MOISTURE
-
U\J/22/90
• • • "* •• •• .. .. .. '
tA-A'✓ER:..G[ VALUE •I-J~-hiOT ANAL"v"7FD HJA!-!"IIERFEREMCES *J-ESTH.~ATED 'w'ALU( '-iJ-PR[SUM?TIVE EVIDENCE OF ~WE~ENCC ot-· MATERIAL •<.-ACTUAL VALUE JS KtJOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS rNOWN TO BE GREATER THAN VALUE GIVEN
•LI-MATERIAL WAS ANAi YZEn FOW ~Lil NOT DElECTED. THE NUMBER IS Tl~E MINIMUM QUANTITATION LIMIT. C-CONFIRMED 9Y GC/MS
1. WHEtJ NO VALUE IS REPORT[O. '.:iEE CHLORDANE CONSTITUFNT'S. 2. CIJf-JSTJTUE~lTS OR f.~ETASOLITES OF TECHNICAL CHLORDANE.
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PESTICIDES/PCB'S DATA REPORT ... SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. .. •• .. ..
• • • • • • • • * • • • • • • • • • • • • • • • • • • • • •
PROJECT NO. 90-785 SAMPLE NO. 48906 SAMPLE TYPE: SOIL • • • . "' . . . . . . "'*•"'*•*••·· .......... . PROG ELEM: SSF CITY: FAYETTEVIL COLLECTION START:
SOURCE: CAROLINA TRANSFORMER STATION ID: 22-SLB
COLLECTED BY: D THOMAN ST: NC 08/07 /90 1120 STOP: 00/00/00
09/19/90
• • • . .. .. .. ..
++• + •• ♦ ••••••••••• * ••••••••• * * "' * •• ,t * ••••• ' ••••••••••••• * •••••••••• ,. UG/KG A/JAL YT I CAL RE SUL TS UG/KG ANALYTICAL RESULTS
..
NA ALDRIN 320U PCB-1232 ( AROCLOR 1232) NA HEPTACHLOR 320U PCB-1248 ( AROCLOR 1248) NA HEPTACHLOR EPOXIDE 320U PCB-1260 ( AROCLOR 1260) NA ALPHA-BHC 320U PCB-1016 (AROCLOR 1016) NA BETA-BHC NA TOXAPHENE NA GAMMA-BHC (LINDANE) NA CHLORDENE /2 NA DELTA-BHC NA ALPHA-CHLORDENE /2 NA ENDOSULFAN I (ALPHA) NA BETA CHLORDENE /2 NA DIELDRIN NA GAMMA-CHLOROENE /2 NA 4.4'-DDT (P,P'-DDTJ NA 1-HYIJt<t)XYCHLORDENE /2 NA 4,4'-DDE (P,P'-DDEl tJA GAr,\',IA-CHLORDANE /2 NA 4,4'-DDD (P,P'-DDDJ NA TRANS-NONACHLOR /2 NA [NORIN NA ALPHA-CHLOROANE /2 NA EtJDOSULFAf,J I I (BETA) NA CIS-NONACHLOR /2 NA ENDOSULFAN SULFATE NA OXYCHLUROANE (OCTACHLOREPOXIDE) /2 NA CHLORDANE (TECH. MIXTURE) /1 NA METHOXVCHLOR 320U PCB-1242 (AROCLOR 1242) NA FIi/ORIN KETONE 320U PCB-1254 (AROCLOR 1254) 32 PERCENT MOISTURE 320U PCB-1221 \ AROCLOR 1221)
•*•REMARKS*••
•••FOOTNOTES•••
•A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-EST!MATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS r,NOWtJ TO BE LESS THAIJ VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•LI-MATERIAL WAS ANALYZED FUR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. C-CONF!RMED BY GC/MS 1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-
-------- - - - ---- - --
PEsl ll:JOES/PCB'S DATA REPORT
+++ •••••••••••• *. * * ••••
" PROJECT NO. 90-785 SAMPLE NO. 48907 ..... SOURC:F.: CAROLIN/\ TR.ll.,NSFORMER
•• STATION ID: 23-SLA
SAMPLE AND AIJALYSIS MANAGF.MHIT ~YSTEM
EPA.-R~GIOM !1! ESD. ATHErJS. GA.
T * T T T t t +
SAMPLE TYPE: SOIL • • • PROG ELEM: SSF COLLECTED
CTT'v': f-AYl:TTEVIL
COLLECTimJ START: CG/07/90
BY: D THOMAN
ST: NC
1i40 STOP: 00/00/00
O;J/22/90 . ' . ... •• .. ..
• * ••
+++ + + • ~ + • + • • t * * * + + * • * • * T * t * T T T * * t t ♦ ~ + + + + • + • + + + * • * * * * * * * + * *TT * T * T * TT*
UG/Y,G
t.JA ALDRIN 1:.:JCOU PCS-1232 \AROCLOR i 232)
NA. HcPIACHLOR I ,3(•0U P'..:~-1 2118 ( 1\ROCLCR 1243)
f,JA HEPTACrlLOF< EPUXIUE 54000 PCB-1260 I AROr,L OR l~Gnl
~.!:'\ !'.U'H!',· BHC 1300U PCB-1016 (AROCLOR 1016)
NA BETA-BHC NA TOXAPHENE
NA GAMMA-BHC ( LI NDANE) NA CHLORDENE /2
NA DEL T .6.-BHC NA ALYHA-CHLORDENE /2
NA ENDOSULFAN I ( Al PHA) "~ BETA Ci-iLORDf.Nf /2
~JI\ DIELDRIN NA GAMMA-CHLORDEtJE /2
rJA cl,4'-P()1 (P.P'-CtQTl NA 1-HYlll·<OXY\...HLOKOfNI:' /2
NA 4.4'-DDE (?.P'-DOE) t" U,~,MMM--CHLORDANE /2 m
NA ~.4'-000 (P,P'-00D) NA fR AM'::,-~!(l~!.ti.r_:HLOR ,,,
1,;A ChiDR IN NA ALPHA-CHLORnANF. i2
~Jf!.. Et~DOSULFAtJ II (BETA) NA CI S-NOWICHLOR /2
NA F:t-.lOOSIJLfM,! SLILf ,ll.1!: NA c,XYCHI. nkLlANI::: l OC. IOC.HLOREPOX !DE) /2
tJA CHLORDANE ( T[CH. MIXTURE) /1 ~~A METHOXYCI !LOR
l ~~OOU PCB-1242 ( AROCLOR 1242) NA ;NIJRJN KE I ONE
50000U PCB-1254 ( AROCLOR 1254) Gl PERCUJT MOiSTURE
1300U PCB-12~1 ( AROCLOR 122i)
• + -1-REMARKS"'"'"'
•••FOOTNOTES••• i-,!.-A\.'E11AGE VALUE 41,JA-NOT ANALY7Fii O,LO.!-!M!ERFERHKES •J-ESTIMATED VALUE *i,;-~R[SUM?TIVE EVIDENCE OF PRESENCE ur MATERIAL
•r.-ACTUAL VALUE IS r.NOWN TO BE LESS THt.lJ VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEtJ •LI-MATERIAL WAS ANALV7f0 FUH ~lll NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. C-CONFIRMED 9Y GC/MS
1. WHEN ~JO VALUE IS REPORT[D, SEE CHLORDANE CONSTITUFNTS L. (OMSTITUENTS OR METABOLITES CF TECHf,JICAL CHLORDANE.
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PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD. ATHENS. GA. 09/19/90 ..
•• •• ..
PROJECT NO. 90-785 SAMPLE SOURCE: CAROL I NA TRANSFORMER STATION ID: 23-SLB
NO. 48908 SAMPLE TYPE: SOIL PROG ELEM: SSF COLLECTED CITY: FAYETTEVIL
COLLECTION START: 08/07/90
BY: D THOMAN ST: NC 1150 STOP: 00/00/00
•• ..
• • • •
••• • • + ♦ • ♦ •••• * •••• * •• * * * ••••• * •• *. * *. * •••••••••• * ••• * •••••••••••••••
UG/KG AIJAL YTICAL RESULTS UG/KG ANALYTICAL RESULTS
NA ALDRW 440U PCB-1232 (AROCLOR 1232) NA HEPTACHLOR 440U PCB-1248 (AROCLOR 1248) NA HEPTACHLOR EPOX!DE 1500 PCB-1260 (AROCLOR 1260) NA ALPHII-BHC 440U PCB-1016 (AROCLOR 1016) NA BETA-BHC NA TOXAPHENE NA GAMMA-BHC (LINDANEJ NA CHLORDENE /2 NA DELTA-BHC NA ALPHA-CHLORDENE /2 NA ENDOSULFAN I (ALPHA) NA BETA CHLORDENE /2 NA DIELDRIN NA GAMMA-CHLORDENE /2 NA 4.4'-DDT \P.P'-DDTJ NA 1-HYIJROXYCHLORDFNF /2 NA 4.4'-DDE (P.P'-DDEl NA GAMMA-CHLORDANE /2 NA 4.4'-DDD (P.P'-DDD) NA TRANS-NONACHLOR /2 NA [NORIN NA ALPHA-CHLOROANE /2 NA ENDOSULFAIJ II (BETA) NA C!S-NONACHLOR /2 NA ENDOSULFAN SULFATE NA OXYCHLORDANE (OCTACHLOREPOXIDE) /2 IJA CHLORDANE (TECH. MIXTURE) /1 NA METHOXYCHLOR 440U PCB-1242 (AROCLOR 1242) NA ENORIN KETONE lOOOU PCB-1254 (AROCLOR 1254) 45 PERCENT MOISTURE 440U PCB-1221 ( AROCLOR 1221)
,,,REMARKS•••
•••FOOTNOTES*•* •A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE 15 KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE 15 KNOWN TO BE GREATER THAN VALUE GIVEN •U-MATERIAL WAS ANALYZED FOP-BUT NOT DETECTED. THE NUMBER IS THE MIIJIMUM QUANTiTATION LIMIT. C-CONFIRMED BY GC/MS 1. WHEN NO VALUE 15 REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-
-- ---- - -- - - - - -- --
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD. ATHENS, GA. ... .. .. .. ..
• • • • • • • • • * * • • • • • • • • • * • • ' * • * • * * PROJECT NO. 90-785 SAMPLE NO. 48909 SAMPLE TYPE: SOIL SOURCE: CAROLINA TRANSFORMER STATION ID: 24-SLA
• • • • • • • • • • • * • • • • • • • • • • • • • • • • •
PROG ELEM: SSF CITY: FAYETTEVIL COLLECTION START:
COLLECTED BY: D THOMAN ST: NC 08/07/90 1205 5 TOP: 00/00/00
-09/19/90
• • • . .. .. .. ..
•• ••+ + •• ♦ ••••••• * • * ••••••• *' • *. * * * • * ••••••••••••••••••••••••••••••••••
UG/KG At,AL YT !CAL RESULTS UG/KG ANALYTICAL RESULTS
NA ALDRIN 1400U PCB-1232 (AROCLOR 1232) NA HEPTACHLOR 1400U PCB-1248 (AROCLOR 1248) NA HEPTACHLOR EPOXIDE 7500 PCB-1260 ( AROCLOR 1260) NA ALPHA-BHC 1400U PCB-1016 (AROCLOR 1016) NA BETA-BHC NA TOXAPHENE NA GAMMA-BHC (LINDANE) NA CHLORDENE /2 NA DELTA-BHC NA ALPHA-CHLORDENE /2 NA ENDOSULFAN I ( ALPHA) NA BETA CHLORDENE /2 NA DIELDRIN NA GAMMA-CHLORDENE /2 NA 4,4'-DDT (P.P'-DDTJ NA 1-HYOSOXYCHLORDENF. /2 NA 4,4' -DDE (P.P'-DDEJ NA GAMMA-CIILORDAN[ /2 NA 4,4'-DDD (P,P'-DDD) NA TRANS-NONACHLOR /2 NA ENDRIN NA ALPHA-CHLOROANF /2 NA ENDOSULF At, I I (BETA) NA CIS-NONACHLOR /2 NA ENDOSULFAN SULFATE NA OXYCHLORDANE (OCTACHLOREPOXIDE) /2 NA CHLORDANE (TECH. MIXTURE) /1 NA METHOXYCHLOR 1400U PCB-1242 (AROCLOR 1242) NA F.NORIN KETONE 7000U PCB-1254 (AROCLOR 1254) 26 PERCENT MOISTURE 1400U PCB-1221 ( AROCLOR 1221 l
•••FOOTNOTES•••
•A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS ~.NOWN TO BE GREATER THAN VALUE GIVEN •U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MWIMUM OUANTITATION LH,HT C-CONFIRMED BY GC/MS 1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
'
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PE,IICJUES/PCB'S DATA REPORT
- - - - -
SAMPLE AND ANALYSIS MANAGfMFNT 5Y5TEM
EP.ll.-P.EGIOM IV ESD. ATHE~JS, CA. --- -
.. ., PROJECT NO. 90-785 SAMPLE NO. 48910 SAMPLE TYPE: ,OIL PROG ELEM: SSF COLLECTED BY: D THOMAN
ST: NC .. .. SOURf.F: f.ARQLINA TRMJSFORMER
STATION JD: 24-SLB
AtJJ\L'1'TICAL RESULTS
NA ALDRIN
NA Ht Pl ACHLOR
1-JA HEPTACHLOI< Ef-'OXfUE
~~:'\ ~1\:._::-: It. ·Sl·IC NA BtlA-BHC NA GAMMA-BHC ( LINDANE) NA DEL T.ti.-BHC
NA ENDOSULFAN I ( Al PHA)
NA DI ELDRBJ NA 4 4 • -nrn '-P, P'-!::iDT)
~JA 4:4•-oDE (F.P'-DDEl NA 4,4'-0DD tP • P' --DDD J
"~ [h.iOR Ii~
~JA ENDO:tt.JLFAN I I (BETA)
NA ft>.!D()51J~_f_ti_M SULF.l'\TE
tJA CHLO~DAfJE (T[CH. r.i!XTURE l /1
6ti!JU PCB-1242 ( AROCLOR 1242)
1500U PCB-1254 <AROCLOR 1 2sa)
660U PCB-1221 (AROCLOR 1221)
•••FOOTNOTES•••
\:iTY: fAYETTEVJL
COLLECTirnJ STA~T: 08/07/90 12i5 STOP: 00/00/00
660Ll PCB--1232 ( AROCLOR 1232)
6f.Ot! Pr..:!3-12118 ( l\ROCLOP. 1248)
1800 PCS-1260 ( AROf.LOR 12/iO)
660U PCB-1016 (AROCLOR 1016)
NA TOXAPHENF NA CHLORDENE /2 NA ALPHA-CHLURDENE /2 ... BEiA vf-iLUttUt:Nt /2 "~ !IIA GAf.\MA-CHLORDENE /2 NA i -t1·v·1·11<1)x Y1_:HLOKOtt-Jt /2 ~JA GAM;.~M-CHLOR.DAiJE /2 NA 1 k' Al\l'::,-!',!(lM,O..f;~L OP. M
NA ALPHA-CHI.OROANI' /2
NA CIS-NONACHLOR /2 NA (J)( YCHi. flf<LJANE ( Qr,T ~r.>iLOREPOX IDE) /2 NA :.~ETHOXYCI :LOR NA rNDR IN rUONE
27 PERC[iJT MOISTURE
•••REMARKS","
--09/22/90
•• .,
• • ••
,-A--AVE~AGE VALVE •i,.;A-NOT ANALY7F.i, •MAl-!NIERFEREMCES •J-EST!MATED VALUE ,:J-PR[St .. H~t=:TIVE EVIDENCE OF F'RFSENCt Ot-MATERIAL
•K-ACTUAL VALUE IS KNO\'IN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN •LI-MATERIAL WAS ANALY7ffl FUH HUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATiON LIMIT. C-CONFIRMED BY GC/MS
1 . WHn~ ~m VALVE IS RE?ORT[D. SEE CHLORDANE CONST I TuFNTS _ L. f_"ONS TI TIJE~JTS OR r.~E TABOL I TES OF TECHtJI CAL CHLORDANE.
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To: Lee Crosby, Chief
Superfund Section
August 30, 1989
From: Bruce Nicholson~µ
Subj: Phase II Sampling Visit For Screening Site Investigation
Toisnot Swamp
Wilson, Wilson County
NCD986166700
On August 29, 1989, Pat DeRosa, David Lilley, and I conducted
Phase II of the Screening Site Investigation at the Toisnot Swamp
Site in Wilson, NC. The site is a stream where sediments were
found by DEM to be contaminated with a coal tar-like substance.
During the Phase I visit conducted August 14, 1989, appropriate
sampling locations and swamp access points were found, and a
subsurface sediment sampling technique was tested. During Phase II
samples were taken at 7 sampling locations to establish the source
and extent of the contamination. The suspected source is a former
coal gasification plant operated by the City of Wilson from about
1920 to 1950.
A small creek that originates at the coal gasification plant
was found to contain oily and tarry substances in sediment. There
were numerous spotty slicks and balls of oil that covered the
surface of the water in this creek even without disturbing the
bottom sediments. This creek enters the main channel of Toisnot
Swamp. Upstream of this entrance point there was no evidence of
tars or oils in sediments or water, downstream of this entrance
point the swamp channel sediments and water were observed to
contain the oils and tars. DEM samples taken in 1988 approximately
0.6 miles downstream of the entrance point show heavy
contamination. During our investigation, small oily slicks were
seen on the banks of Toisnot Swamp, 4 miles downstream of the
discharge point.
Two sediment samples were taken in the discharge creek
originating at the coal gasification plant, one was taken upstream
of where this discharge creek enters Toisnot Swamp, and two were
taken downstream of this point (80 yards and 4 miles downstream
respectively). Surface water samples were taken at these points
also. In addition, a subsurface soil sample was taken from the
gasification plant property from a swale that appeared to be in the·-
flow path for surface drainage from the plant building into the
discharge creek. All samples will be analyzed for organic, and
inorganic constituents.
BIN\mem\toistrp2
cc: Grover Nicholson
-- -- - - - - - - - - - - - - --SAMPLE AND ANALYSIS MANAGEMEMT SV5TfM
EP.ti.-REG!OM IV ESD, ATHE~~S. CA.
PESl!CIOES/PCB'S DATA REPORT ... ..
•• .. ..
♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ ♦ * ♦ ♦ ♦ ' T T 1= ~ $
PROJECT NO. 90-785 SAMPLE NO. 48911 SAMPLE TYPE: SOIL
SOUR CF: CAROL I NI\ TRM!SFORM!:R STATION ID: 25-SLA
• • • PROG ELEM: SSF COLLECTED CITY: fAYtTTEVIL
COLLECTICtJ STA~T. OG/07/90
BY: D THOMAN ST: NC
1140 STOP: 00/00/00
09/22/90
' . ' ". •• ..
• •
..-.;.+ ♦ + • • • ♦ • ♦ • * lJ. * * :t. • ♦ * • ♦ • • ♦ 'f T 1' T :t-♦ :r ♦ 1= ,1. ♦ <I-"-♦ • ♦ ♦ ♦ IJ • • ♦ ♦ ♦ ♦ * • ♦ * ♦ ♦ * ♦ * F T * * 1 ♦ "fT ♦
UC/:<C :..tJML','TICAL RESULTS 1•1G/!1'.G A~~AL. \'TIC,'..L rzc:.:.n .. TS
N"-ALDRIN 1300\J PCB-·1232 ( AKOCLOR i 232)
N/1 HEP f.ACHLOR 1 :1(H)I I PCB-1218 ( :'\P.OCLCP. 1248)
!~A HEPTACHLOR Ei'OXI DE 26000 PCB-1260 (AROCLtiR 1'.2G0)
~J:\ :\!...r?:A·-SIIC 1300U PCB-1016 (AROCLOR 1016)
NA BtlA-BHC NA TOXAPHENF
NA GAMMA-OHC ( LINDANE l NA CHLORDENE /2
NA DEL T.O.-BHC NA Ali'HA-CHLORDENE /2
NA ENDOSULFAN I (ALPHA) ~..:A 5ETA CMLORDF.NE /2
NJ\ DIE~DRltJ NA GAMMA-CHLOROE~JE /2 NA "1_4:-11!)1 1Y. ~•-DDT) NA 1-H,'flKl).ltYCHLOkDfNf /2 NA 4.4'-DDE (P.P'-DDEJ ~~A GAr,~MA-CHLOROAI-JE /2
NA 4.4'-0DD {P,P'-0D0) NA I WAM,S-!',-!(l!-,!,O.J_.HLQR 10 .. ~ Li.JUR. i N NA ALPHA-CHLOROANF /2
NA ENDO~UL F A~J II {BETA) NA CIS-NONACHLOR /2
NA f: NDOSI.IL f ,O,M SULF/\TE NA t)x VCHI_ t'lf<llANE tOC:TbCHLOREPOXIOE) /2
tJA CHLORD,\NE {T[Ci-1. MIXTURE) / 1 ~~A METH:JXYC! ILOR
1 :"i!J(JU P(B-1242 UROCLOR 1242) NA f NIJR IN HIONE
25000U PCB-1;>54 (AROCLOR l "?.S<l l GC) PERCENT MOISTURE
130QU PCB-1221 (1-ROCLOR 1221)
•••REMARKS•••
•••fOOTNOTEC..••• TA-AVERAGE V:..LVE •1-.iA-NOT ANALYLEr, HIO.l-!MIERfERE!'-lCES •..!-ESTIMATED VALUE ic:~-?RESUM?TiVE EVIVENCE OF ~RESENCI: ur MATERlAL •K-A.CTLIAL VALUE IS Y,NOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE 15 ,.NOWN TO BE GREATER THAN VALUE GIVElJ
+Li-MATERIAL WAS ANAl ·v7FO FOK t\tll NOT D!:!ECTED. THE ~JUM8ER IS THE MH~IMUM QUAi-JiITATION LiMIT. C-CONFIP.MED 9Y GC/MS
1. WHHJ ~JO VALUE rs RE?ORT[D. SEE CHLOiWANE CONSTiTUFNTS 2. CO!--!S1"JTl_!~~~TS CR METABOLITES OF TECHtJICAL CHLORDANE.
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--·-· -- --
PESTIC!DES/PCB'S DATA REPORT
- - - - -SAMPLE AIJD ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. --- - -
... .. .. .. ..
............ **** • • • • • * * * • • • • * * ' • • • "' * • ' " • * * • • • • • • • • • • • • PROJECT NO. 90-785 SAMPLE SOURCE: CAROL I NA TRANSFORMER STATION JD: 25-SLB
NO. 48912 SAMPLE TYPE: SOIL PROG ELEM: SSF CITY: FAYETTEV!L COLLECTION START:
COLLECTED BY: D THOMAN ST: NC 08/07/90 1150 STOP: 00/00/00
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09/19/90 ...
•• .. .. .. ♦♦+ + • + • ♦ •• * •••• * • * •••• * •• * • * * * * * * * • * * ••••• * •••••••••••••••• * * * * •• *** UG/KG AIJAL YT I CAL RESULTS UG/KG ANALYTICAL RESULTS
NA ALDRIN 400U PCB-1232 (AROCLOR 1232) NA HEPTACHLOR 400U PCB-1248 (AROCLOR 1248) NA HEPTACHLOR EPOX !DE 2000 PCB-1260 ( AROCLOR 1260) NA ALPHA-BHC 400U PCB-1016 (AROCLOR 1016) NA BETA-BHC NA TOXAPHENE NA GAMMA-BHC (LINDANE) NA CHLORDENE /2 NA DELTA-BHC NA ALPHA-CHLORDENE /2 NA ENDOSULFAN I ( ALPHA) NA BETA CHLORDENE /2 NA D!ELDRJN NA GAMMA-CHLORDENE /2 NA 4.4'-DDT (P,P'-DDT) NA 1-HYDROXYi:HLORDENE /2 NA 4,4'-DDE (P.P'-DDE) NA GAMMA-CllLORO,\t.JE /2 NA 4,4'-DDD (P,P'-DDD) NA TRANS-NON.ACHLOR /2 NA [NORIN NA ALPHA-CHLORnANF /2 ~JA EtJDOSULF AN I I (BETA) NA CJS-NONACHLOR /2 NA ENDOSULFAN SULFATE NA OXYCHLORDANE (OCTACHLOREPOXIDE) /2 NA CHLORDANE ( TECH. MIXTURE) /1 NA METHOXYCHLOR 400U PCB-1242 (AROCLOR 1242) NA FNORIN ~ETONE 1500U PCB-1254 (AROCLOR 1254 J 43 PERCENT MOISTURE 400U PCB-1221 l AROCLOR 1221)
•••REMARKS-'*•
•••FOOTNOTES•••
•A·-AVERAGE VALUE • NA-NOT ANALYZED •NA 1-1 NTERF ERENCES • J-EST !MATED VALUE • N-PRESUMPT I VE EV !DENCE OF PRESENCE OF MA TERI AL •K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN •U-MATER!AL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. C-CONFIRMED BY GC/MS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
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