NCD095458527_20000425_FCX Inc. (Statesville)_FRBCERCLA RA_Underground Storage Tank Soil Contamination Report-OCR

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Work Order No. 20064-025-100-6020
RECEIVED
JUN 3 0 2000
-~· ~. ,rUND SECTION
UNDERGROUND STORAGE TANK
SOIL CONTAMINATION REPORT
FORMER FARMERS COOPERATIVE EXCHANGE, INC.
STATESVILLE, NC 28677
Prepared For
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT & NATURAL RESOURCES
Mooresville Regional Office
919 North Main Street
Mooresville, NC 28115
Prepared By
ROY F. WESTON, INC.
1625 Pumphrey Ave.
Auburn, Alabama 36832-4303
25 APRIL 2000
K:\2006.J\025160·10\UST-CLSR\FCX-SCR.DOC 2,1 April 2000\'crsion
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TABLE OF CONTENTS
SECTION I GENERAL INFORMATION .............................................................................. 1-I
SECTION 2 SITE UST HISTORY ........................................................................................... 2-I
SECTION 3 SITE INVESTIGATION ...................................................................................... 3-I
SECTION 4 CONCLUSION ..................................................................................................... 4-1
APPENDIX A FIGURES
APPENDIX B ANALYTICAL RESULTS
APPENDIX C CHAIN-OF-CUSTODY FORM
LIST OFT ABLES
Table 2-1 Summary of Tank Specifications and History .................................................................. 2-2
Table 3-1 Soil Analytical Results ..................................................................................................... 3-2
K:12006'1'025160-HhlJST-CLSR\l'CX-SCR.DOC 2·1 April 2000 Version
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SECTION 1
GENERAL INFORMATION
Farmer's Cooperative Exchange, Inc. (FCX) filed a voluntary petition under the prov1s1ons of
Chapter 11 of the United States Bankruptcy Code on September 17, 1986. At that time, the U.S.
Environmental Protection Agency (EPA), North Carolina Department of Environment and Natural
Resources, and FCX entered into an agreement, whereby FCX established a trust to be used to
remcdiatc pesticide contamination at the site. The site (Figure I; Appendix A) was proposed for
inclusion on the National Priorities List (NPL) on June 24, 1988 and was finalized on the NPL on
February 21, I 990.
FCX owned and operated the two underground storage tanks (USTs) from the mid-I 960s until
1986. The following addresses were on record for the Statesville site during the time of operation
prior to closure:
Site Address and UST location:
FCX, Inc. (distribution center)
I 620 West Front Street
Statesville, NC 28677
Horne Office Address (former)
FCX, Inc.
P.O. Box 2419
Raleigh, NC 27602
The tanks were abandoned prior to 1988 and arc therefore not directly subject to the UST regulatory
requirements. Therefore, no state facility identification number is available. However, since the
site has been listed under CERCLA, an EPA identification number has been issued. The EPA
Facility I.D. number for the site is: NC095458527.
K:1200(,.l\02W,0-\0\1 !Sl-Cl.~RIFCX-SCR.D<JC 24 April 2000 Version 1-1
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SECTION 2
SITE UST HISTORY
Responsibility for the site was accepted in 1990 by the U.S. Environmental Protection Agency
(EPA) due to the discovery of pesticide. Remediation activities are being conducted by the EPA
Region IV office in Atlanta, Georgia. The primary contacts for the project arc:
USEPA Region IV
Remediation Project Manager
ERRS Contractor
(closure contractor)
ARCS Consultant
North Carolina DENR Manager
Analytical Laboratory for Soil
Contamination Report Data
Mr. McKenzie (Ken) Mallary
USEPA Region IV
Atlanta Federal Center
61 Forsyth Street, SW
Atlanta, GA 30303-3104
CMC, Inc.
1151 Jessamin Station Pike
Nicholasville, KY 40356
Proj. Manager: Mr. Rick Hollingsworth
Roy F. Weston, Inc.
Suite 200
5405 Metric Place
Norcross, GA 30092-2550
Proj. Scientist: Mr. Bret Missildine
Mr. Nile Testerman
Division of Waste Management
40 I Oberlin Road, Suite 150
Raleigh, NC 27605-1350
Prism Labs, Inc.
449 Springbrook Road
Charlotte, NC 28224
NC Certification# 402
FCX -Statesville was a distribution center for farm chemicals, fertilizers, and agricultural seeds. In
1988, the facility was closed and abandoned at which time the tanks were emptied and taken out-of~
service. Historical information indicates the USTs supplied fuel primarily for company delivery
trucks and yard vehicles. Table 2-1 presents a summary of tank specifications for the identified
USTs.
K:\200(,,11025160,HhUST-CI.SR\FCX-SCR.DOC 24 April 2000 Vcrsinn 2-1
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SITE UST HISTORY
TABLE 2-1
SUMMARY OFT ANK SPEC I FICA TIO NS AND HISTORY
Tank No. Install Date Size (Gal.) Dimensions I Last Date I
Contents Removed :
' ' ca. 1965 7 ft (dia.) x 20 ft. ' I I 7,500 ! Gasoline 11 May 1999 .
'
'"" __ ... ,. ______ ·--·---·----..
! I : I 2 ca. 1965 10,000 7 ft (dia.) x 26 Ii. i Diesel 11 May 1999
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During the remedial activities at the site, EPA and NCDENR requested that the USTs be removed from the ground. CMC, Inc. (CMC) along with WESTON performed the removal in May of 1999 and in accordance with State requirements, submitted an Underground Storage Tank Closure Report for the si tc.
Laboratory analysis of the samples indicated slight contamination in the vicinity of the pump island, and along both product lines. Based upon the closure guidelines, CMC and WESTON were asked to conduct additional excavation of the effected areas, perform requisite sampling, and submit the samples for analysis using the extended sampling procedures (EPA 8260 and MADEP-VPH; EPA 8270 and MADEP-EPH). Based upon the sample results and limited excavation necessary to meet the required MCLs, it is estimated that the quantity released was less than twenty (20) gallons total.
Original sample locations, analyses, and report results may be found in the UST Closure Report dated 9 July 1999, which is included in this report by reference.
K·'200(,.l\0251t,O,IO\UST-CLSRIFCX-SCK.DOC 2.J April :2000 Vmion 2-2
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SECTION 3
SITE INVESTIGATION
The excavation act1v1t1es included removal of the small, concrete pump island (20 square feet).
Sampling or the additional soil in the area of the pump island and product lines involved removing
an additional three feet of soil from the effected areas and placing it on a stockpile area. As
previously discussed in the Closure Report, the product lines were approximately 1.5 feet below
ground surfoce (bgs) and 1.5 feet in width. The additional excavation performed to remove the
contaminated soil made the two product line trenches approximately 2.5 feet wide and a total of 4.5
feet bgs. The soil stockpile was previously established as a result of the on-going USEPA pesticide
remediation activities at the site.
Soil samples were obtained in accordance with North Carolina Department of Environment and
Natural Resources (NCDENR) Groundwater Section "Guidelines for the Investigation and
Remediation of Soil and Groundwater" for petroleum USTs. One grab sample each was taken from
beneath the former pump island location and from beneath the product line for Tank No. I. Two
grab samples were collected beneath the associated product line for Tank No. 2. Figure 2
(Appendix A) shows the location of these four sample points relative to the former tanks and
buildings.
Soil samples were taken from near the bottom of the excavated area, immediately placed in labeled
glass containers, scaled, and placed into a sample cooler. At no time during the excavation was
groundwater encountered. Therefore, groundwater samples were not required for this investigation.
The samples were identified using the previous UST Closure Report sample nomenclature modified
to indicate the current sample event.
Soil sampling was performed by Mr. Eric Crisp of WESTON and the samples were delivered to
Prism Labs the same day. All samples were analyzed using the Massachusetts Department of
Environmental Protection (MADEP) procedure (VPH and EPA 8260/EPH and EPA 8270) in
accordance with North Carolina Department of Environment and Natural Resources (NCDENR)
Groundwater Section Guidelines. Table 3-1 presents the analytical results of the sampling
activities. The laboratory reports are provided in Appendix B. Because no groundwater was
encountered, Soil-to-Groundwater maximum concentration limits (MCLs) were used in the
interpretation or the results.
K:;200(,.l'025160·I01!JST-CLSR\FCX-SCR.DOC 2,1 Ap1il 2000 Vc1sion 3-1
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SITE INVESTIGATION
TABLE3-l
SOIL ANALYTICAL RESULTS
Compound Sample ID
FCX-61-A FCX-7GL-A FCX-8D L-A FCX-9D L-A
C5-C8 n.d. n.d. n.d. n.d.
C9-C 18 n.d. n.d. n.d. n.d.
19-C36 n.d. n.d. n.d. n.d.
Accnaphthenc n.d. n.d. n.d. n.d.
Accnaphthylcnc n.d. n.d. n.d. n.d.
Anthraccnc n.d. n.d. n.d. n.d.
n.d. n.d. n.d. n.d.
C9-C22 n.d. n.d. n.d. n.d.
Benzene n.d. n.d. n.d. n.d.
13cnzo( a )anthraccnc n.d. n.d. n.d. n.d.
13cnzo(b )lluoranthcnc n.d. n.d. n.d. n.d.
13cnzo(g,h,i )pcry I cne n.d. n.d. n.d. n.d.
13cnzo( K) 11 uoranthenc n.d. n.d. n.d. n.d.
13cnzo( a )py rcnc n.d. n.d. n.d. n.d.
n-Butylbcnzcnc n.d. n.d. n.d. n.d.
sec-13utylbenzcnc n.d. n.d. n.d. n.d.
tcrt-13utylbcm:ene n.d. n.d. n.d. n.d.
n-Propylhcnzcnc n.d. n.d. n.d. n.d.
Chromium 81 mg/kg 86 mg/kg 82 mg/kg 53 mg/kg
Chryscnc n.d. n.d. n.d. n.cl.
Di bcnz( a,h )anthracenc n.d. n.d. n.d. n.d.
1.2-Dichlorobcnzcne n.d. n.d. n.d. n.d.
1,3-Dichlorohenzcne n.d. n.d. n.d. n.cl.
1.4-Dichlorobcnzcne n.d. n.d. n.d. n.cl.
I, 1-Diehlorocthane n.d. n.d. n.d. n.cl.
K:'-.:'006.1-..p::51t,0,10\lJ~T-Cl,SRIFCX-SCk.DOC ~~ April 2000 Version 3-2
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SITE INVESTIGATION
TABLE3-l
SOIL ANALYTICAL RESULTS
Compound Sample fD
FCX-61-A FCX-7GL-A FCX-8DL-A FCX-9DL-A
1,2-Dichloroethanc n.d. n.d. n.d. n.d.
( ethylene dichloride)
1,2-Dichlorocthene (cis) n.d. n.d. n.d. n.d.
1,2-Dichloroethcnc (trans) n.d. n.d. n.d. n.d.
1.1-Dichlorocthylene n.d. n.d. n.d. n.d.
1,2-Dichloropropane n.d. n.d. n.d. n.d.
1,3-Dichloropropene (cis & trans) n.d. n.d. n.d. n.d.
Ethylcbcnzcne n.d. n.d. n.d. n.d.
Fluoranthcnc n.d. n.d. n.d. n.d.
Fluorcnc n.d. n.d. n.d. n.d.
lndeno( 1.2,3-cd)pyrenc n.d. n.d. n.d. n.d.
I sopropy I benzene n.d. n.d. n.d. n.d.
lsopropyl ether n.d. n.d. n.d. n.d.
(di-isopropyl ether)
Lead 23 mg/kg 22 mg/kg 20 mg/kg 15 mg/kg
2-Mcthylnaphthalene n.d. n.d. n.d. n.d.
Methyl ethyl tert-butyl ether n.d. n.d. n.d. n.d.
Naphthalene n.d. n.d. n.d. n.d.
Phcnanthraccnc n.d. n.d. n.d. n.d.
Pyrenc n.d. n.d. n.d. n.d.
1.2.4-Trimethylbenzcnc n.d. n.d. n.d. n.d.
1,3,5-n.d. n.d. n.d. n.d.
Toluene n.d. n.d. n.d. n.d.
Xylencs (mixed) n.d. n.d. n.d. n.d.
n.d. ~ not detected
t,,:-\:'[10(d'02Slf,0HhUST-CLSRIFCX-SCR.DOC 2:.J ,\pill 2000 Version 3-3
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SITE INVESTIGATION
No groundwater sampling was performed as a result of this investigation because no groundwater
was intercepted. Water table depths at the site arc approximately 25 feet bgs.
The excavated soil material was stockpiled with soils already stored on site that arc being treated as
a part of the of the ongoing remediation of pesticides in the soil at the facility. The material will be
thermally treated using Base Catalyzed De-sorption (BCD) and used for backfill on the property.
Industrial Recovery Systems, Inc. is the contractor performing the process. The permitting of the
thermal units has taken into account the potential for petroleum products in the soil.
K:\~006,l'-0251(,0..!0,IJS"l-CLSR\FCX-SCIU)OC 2·1 April 2000 Version 3-4
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SECTION 4
CONCLUSION
During the field work, it was observed that the side walls and base of the excavated area was well
within the unsaturated zone. Additionally, it would appear that the small amount of contaminated soil
in the vicinity of the product lines and pump island was successfully removed, based upon the data
collected during the soil contamination investigation for the two USTs. It also appears that no impact
to the site groundwater has occurred as a result of past operation of the former UST systems.
As a result, WESTON requests that a letter of"no further action" be issued for the underground storage
tanks formerly used at the site.
K ··.~001,.1102~1(,().!{)·,lJ~T-CI.SR\f:CX-SCR.DOC 2·1 April 2000 Version 4-1
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APPENDIX A
FIGURES
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-Q,
J
~ ·'-"'-''"'' --
'"'
;:,~J"':.];t ~~~ -
!
~ -:::1 ( . ~ , •II~~ I'\ I' , , •~;.,-,, l
1 SCALE 1:24 000
======ai:'=E=aa:::::::=:E==1:=0E==ee==ee==e'==e'==ee==e'==e'==e'==ee==e'==e'~l MILE
1000 0 1000 2000 3000 5000
CONTOUR .INTERVAL 10 FEET
NATIONAL GEODETIC VERTICAL DATUM OF 1929
A Portion of the U.S.G.S. 7.5 Minute
West Statesville, North Carolina
Map Showing the General Location
of the Subject Property.
FCX -Statesville, North Carolina
K.:11uuo4101511iu4u1us·r:cLSR\FJGPAGE.ooc
6000 7000 FEET
Project: 20064.025.100
U.S. EPA
25 April 2000
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RW
□
UPPER WAREHOUSE LOWER WAREHOUSE
1---7
FCX-lPH-4
FCX-lPH-2
I ~ ~ FCX-1PH-7GL
, ...,--rcx-7Gt-A
2.5' (TYPICAL)--'--l T1 FCX-61-A
I ls: I ~o FCX-lPH-3 I FCX-lPH-61
FCX-8DL-A
FCX-1PH-8DL k I / -,j(~FCX-9DL-A
\ __l --I rcx~ 1PH-9DL -------r --~--1 □ RW
I
I 2.5' (TYPICAL>---'-
1
----l ------T2 I o.,..--I 26'
MW
I I [.'.CX-lPH-5 ___ FCX-lPH-1 ____ j
4
MW
&
pp
0
SIDEWALK
W FRONT STREET
SITE PLAN -SOIL CONTAMINATION REPORT
NOT TO SCALE
MW
&
STORM DRAIN
..
□ RW
pp
SAMPLE MADEP
(mg/kg)
FCX-6I-A BA
FCX-7GL-A BA
FCX-BDL-A BA
FCX-9DL-A BA
BA -BELOW ACTION LEVEL
E0CAVATION DETAIL
NOT TO SCALE
SAMPLE DRO/GRO
(mg/kg)
FCX-TPH-1 BDL
' FCX-TPH-2 BDL
FCX-lPH-3 BDL
FCX-lPH-4 BDL
FCX-lPH-5 BDL
FCX-lPH-6I 420/BDL
FCX-1PH-7Gl 26/BDL
FCX-1PH-8DL . 13/BDL
FCX-1PH-9DL 21/BDL
BDL -BELOW REPORTABLE DElECTION LIMIT
.... as a
VJ z
0
F <( u 0 ...J
w ...J
0...
2
<(
VJ
0 z
3
0
I
VJ
z ·<(
...J
0...
DWG. NO.
200M-02&--100-f040
SHEET OF
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K:\200641025\6040\UST-CLSRIFCX-SCR.DOC 24 April 2000 Version
APPENDIX 8
ANALYTICAL RES UL TS
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Lab Report
2/9/2000
Roy F. Weston, Inc
Ralph McKeen
5404 Metric Place
Norcross, GA 30092
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Lab Submittal Date/Time:
Full Se,vice Analy1ical & Environmental Solutions
Page 1 of 25
FCX-OU2-Remedial Action
FCW-9D L-A
AB56490
AO24F5
1/27/2000 10:55
1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST METHOD DATE/TIME
PARAMETER RESULT UNITS MDL REFERENCE STARTED ANALYST -----------------------------------------
METALS DIGESTION METHOD 3050
PREP. METHOD 3550
CHROMIUM, TOTAL
LEAD, TOTAL
CS-CB Aliphatics
C9-C12 Aliphatics
C9-C 10 Aromatics
Surrogate% Recovery -PIO
Surrogate % Recovery -FtD
Dilution Factor
Dry Weight Received
EXTRACTION FOR EPH
C9-C18 ALIPHATICS
C19-C36 ALIPHATIC$
C11-C22 AROMATICS
SURROGATE RECOVERY -ALIPHATIC
SURROGATE RECOVERY· AROMATIC
SURR:2-BROMONAPHTHALENE
SURR:2-FLUOROBIPHENYL
DILUTION FACTOR
DRY WEIGHT
CALCULATIONS BASED ON DRY WT
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
Completed
Completed
53
15
Not detected
Not detected
Not detected
74
86
12. 79 g
Completed
Not detected
Not detected
Not detected
53
121
113
112
8.0 g
80
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
%
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
%
%
%
mg/kg
mg/kg
% DRY WT.
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.0
1.0
7
6
2
3050
3550
6010
6010
MADEP VPH
MADEP VPH
MADEP VPH
(70-130) MADEP VPH
(70-130) MADEP VPH
MADEP VPH
MADEP VPH
40
20
100
MADEP-EPH
MADEP-EPH
MADEP-EPH
MADEP-EPH
(40-140) MADEP-EPH
(40-140) MADEP-EPH
(40-140) MADEP-EPH
(40-140) MADEP-EPH
0.01
6.0
6.0
6.0
6.0
6.0
12.0
MADEP-EPH
MADEP-EPH
SM 2540 G
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
2/8/2000 08:00 GRR
1/2812000 08:00 JDP
2/8/2000 16:01
2/8/2000 16:01
1/28/2000 22:08
MSP
MSP
KV
1/28/2000 22:08 KV
1/2812000 22:08 KV
1/2812000 22:08
112812000 22:08
1128/2000 22:08
1/28/2000 22:08
KV
KV
KV
KV
1/31/2000 08:00 JDP
2/412000 01 :20
2/4/2000 01 :20
214/2000 01:20
2/4/2000 01 :20
2/4/2000 01 :20
2/412000 01 :20
2/4/2000 01 :20
2/4/2000 01 :20
2/4/2000 01 :20
2/1/2000 09:00
DMM
DMM
DMM
DMM
DMM
DMM
DMM
DMM
DMM
GAM
1/27/2000 20:04 CMS
1/2712000 20:04 CMB
1/2712000 20:04 CMB
1/27/2000 20:04 CMS
112712000 20:04 CMB
1/27/2000 20:04 CMB
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
•l-+9 ~prin~brook l\o.Hl .... P.O. Btn 2-105,t.1 .... Chulotil', i\'C 2tl22 ➔-0~-D
l'lwnc: -;"(l,1/529-h~h•I .... Toi! Fn•c :'\umber: 1-800/5:!9-h::;fi-l _.... F,n: 7(1.J/S25-ll-l0'/
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lab Report
2/9/2000
Roy F. Weston, Inc Customer Project ID:
Ralph McKeen Customer Sample ID:
5404 Metric Place Prism Sample ID:
Login Group: Norcross, GA 30092 Sample Collection Date/Time:
Lab Submittal Date/Time:
:t.·'
'•INC -~>.
Full Service Analyl1cal & Environmental Solutions
Page 2 of 25
FCX-OU2-Remedial Action
FCW-9D L-A
AB56490
AO24F5
1/27/2000 10:55
1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST METHOD DATErrlME
PARAMETER RESULT UNITS MDL REFERENCE STARTED ANALYST
N-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
SEC-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
TERT-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
CARBON TETRACHLORIDE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
CHLOROBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
CHLORODIBROMOMETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
CHLOROETHANE Not detected ug/kg 12.0 SW846-8260 1/27/2000 20:04 CMB
CHLOROFORM Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
CHLOROMETHANE Not detected ug/kg 12.0 SW846-8260 1/27/2000 20:04 CMB
2-CHLOROTOLUENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
4-CHLOROTOLUENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
1,2-DIBROMO-3-CHLOROPROPANE Not detected ug/kg 12.0 SW846-8260 1/27/2000 20:04 CMB
1,2-DIBROMOETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
DIBROMOMETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
1,2-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
1,3-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
1,4-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMS
DICHLORODIFLUOROMETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMS
1, 1-DICHLOROETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
1,2-DICHLOROETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
1, 1-DICHLOROETHENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
CIS-1,2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20 04 CMB
TRANS-1,2-DICHLOROETHENE Nol detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMS
1.2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
1,3-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260 1/2712000 20:04 CMB
2,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
1, 1-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
ETHYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
HEXACHLOROBUTADIENE Not detected ug/kg 6.0 SW846-8260 1127/2000 20 04 CMB
ISOPROPYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/2712000 20 04 CMB
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
H'l Springbrook. l\nad ,-l'.0. Bo, 2-Hl5➔3-. Ch.nlotll'. NC 2H22-Hl5➔:-
l'horH" 70..Jf.t;2LJ-h'\H -. Toll hl't' :\.'u1nbL'r: 1-800/529-b]b..j-. F.1,: 70--l/52~-{l .. HJLJ
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Lab Report
2/9/2000
Roy F. Weston, Inc
Ralph McKeen
5404 Metric Place
Norcross, GA 30092
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Lab Submittal Date/Time:
Full Service Analy1,c,11 & Environmontal Sol11tions
Page 3 of 25
FCX-OU2-Remedial Action
FCW-9D L-A
AB56490
AO24F5
1/27/2000 10:55
1/27/2000 14:20
The following analy1ical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST METHOD DATE/TIME
PARAMETER RESULT UNITS MDL REFERENCE STARTED ANALYST
P-ISOPROPYLTOLUENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
METHYLENE CHLORIDE Not detected ug/kg 120.0 SW846-8260 1/27/2000 20:04 CMB
NAPHTHALENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
N-PROPYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
STYRENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
1.1.1.2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMS
1.1.2,2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMS
TETRACHLOROETHENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMS
TOLUENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMS
1.2,3-TRICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMS
1.2.4-TRICHLOROBENZENE Not detected ug/kg 6.0 SWB46-8260 1/27/2000 20:04 CMS
1.1, 1-TRICHLOROETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMS
1.1.2-TRICHLOROETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMS
TRICHLOROETHENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMS
TRICHLOROFLUOROMETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMS
1.2.3-TRICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMS
1.2.4-TRIMETHYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMS
1,3,5-TRIMETHYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMB
VINYL CHLORIDE Not detected ug/kg 12.0 SW846-8260 1/27/2000 20:04 CMB
TOTAL XYLENES Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMS
2-BUTANONE (MEK) Not detected ug/kg 60.0 SW846-8260 1/27/2000 20:04 CMS
2-CHLOROETHYL VINYL ETHER Not detected ug/kg 12.0 SW846-8260 1/27/2000 20:04 CMS
4-METHYL-2-PENTANONE (MIBK) Not detected ug/kg 60.0 SW846-8260 1/27/2000 20:04 CMS
ACETONE Nol detected ug/kg 120.0 SW846-8260 1/27/2000 20:04 CMS
CARBON DISULFIDE Nol detected ug/kg 120.0 SW846-8260 1/27/2000 20:04 CMS
VINYL ACETATE Not detected ug/kg 60.0 SW846-8260 1/27/2000 20:04 CMS
CIS-1.3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMS
TRANS-1,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMS
2-HEXANONE Not detected ug/kg 60.0 SW846-8260 1/27/2000 20:04 CMS
IPE Not detected ug/kg 6.0 SW846-8260 1127/2000 20:04 CMB
NC Certificalion No. 402 -SC Certificalion No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
.J.lll Sp,inghrnols l{11,1d .... P.O. Bel\ ~.JO:i-1.1 .-. Ch.n!otll', ~C :!822-1-0:i-l>
l'lw1H': :"(l--t/,;:!Y-b."~h-1 -.. Toll he,· :'\umlH'r: 1-1:H)0/524-ti3h➔--. F,n: 70-1/:;~;i-0-lllO
--------~-----··-·--·
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Lab Report
2/9/2000
Roy F. Weston, Inc Customer Project ID:
Ralph McKeen Customer Sample ID:
5404 Metric Place Prism Sample ID:
Login Group: Norcross, GA 30092 Sample Collection Date/Time:
Lab Submittal Date/Time:
V M
'S?tNC . . ,
t·
Full SeN1ce Analyt1cul & Environment.ii Solutions
Page 4 of 25
FCX-OU2-Remedial Action
FCW-9D L-A
AB56490
A024F5
1/27/2000 10:55
1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST METHOD DATEfTIME
PARAMETER RESULT UNITS MDL REFERENCE STARTED ANALYST
MTBE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:04 CMS
SURR:DIBROMOFLUOROMETHANE 85 % 70-130 SW846-B260 1/27/2000 20:04 CMS
SURR:TOLUENE-DB 90 % 70-130 SW846-8260 1/27/2000 20:04 CMB
SURR:BROMOFLUOROBENZENE 79 % 70-130 SW846-8260 1/27/2000 20:04 CMS
----------
ACENAPHTHENE Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
ACENAPHTHYLENE Not detected ug/kg 410 SWB46-8270 2/2/2000 15:21 HWC
ANTHRACENE Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
BENZO(A)ANTHRACENE Not detected ug/kg 410 SW846-8270 2/212000 15:21 HWC
BENZO(B)FLUORANTHENE Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
BENZO(K)FLUORANTHENE Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
BENZO(A)PYRENE Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
BENZO(GHl)PERYLENE Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
BIS(2-CHLOROETHOXY)METHANE Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
8IS(2-CHLOROETHYL)ETHER Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
BIS(2-CHLOROISOPROPYL)ETHER Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
BIS(2-ETHYLHEXYL)PHTHALATE Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
4-BROMOPHENYL PHENYL ETHER Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
BUTYL BENZYL PHTHALA TE Not detected ug/kg 410 SWB46-8270 2/2/2000 15:21 HWC
4-CHLORO-3-METHYLPHENOL Not detected ug/kg 410 SW846-8270 2/212000 15:21 HWC
2-CHLORONAPHTHALENE Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
2-CHLOROPHENOL Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
4-CHLOROPHENYL PHENYL ETHER Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
CHRYSENE Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
DIBENZO(A.H)ANTHRACENE Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
DIBENZOFURAN Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
DI-N-BUTYLPHTHALATE Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
1.2-DICHLOROBENZENE Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
1.3-DICHLOROBENZENE Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
1.4-DICHLOROBENZENE Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
➔-l!J ~pringhrrnik RoJd .... P.O. l\p\ 2➔0:i..J.,-. Ch.nlolll', KC 2H22-l-O:i-l:;
l'll(l!ll': "'.'ll..J624-h.,h-l .... Tnll Frt.'t' ~umh.•r: !-H0tl/52q-t,Jh-t .... F,n: 70.t/_::.25-0-t(lY
I
Lab Report
I f-ull Seivice Analytic;il & EnvironmlJ11tal Solutions
I 2/9/2000 Page 5 of 25
Roy F. Weston, Inc Customer Project ID: FCX-OU2-Remedial Action
Ralph McKeen Customer Sample ID: FCW-9DL-A
D 5404 Metric Place Prism Sample ID: AB56490
Login Group: AO24F5 Norcross, GA 30092 Sample Collection Date/Time: 1/27/2000 10:55
D Lab Submittal Date/Time: 1/27/2000 14 20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
m TEST TEST METHOD DATE/TIME
PARAMETER RESULT UNITS MDL REFERENCE STARTED ANALYST
I 2,4-0ICHLOROPHENOL Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
DIETHYL PHTHALATE Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
2,4-0IMETHYLPHENOL Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
I DIMETHYL PHTHALATE Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
2.4-DINITROPHENOL Not detected ug/kg 2050 SW846-8270 21212000 15:21 HWC
2,4-0INITROTOLUENE Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
I 2,6-DINITROTOLUENE Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
0I-N-OCTYLPHTHALATE Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
FLUORANTHENE Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
I FLUORENE Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
HEXACHLOROBENZENE Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
I HEXACHLOROBUTADIENE Nol detected ug/kg 410 SW846-8270 21212000 15:21 HWC
HEXACHLOROCYCLOPENTADIENE Nol detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
HEXACHLOROETHANE Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
I INOEN0(1.2 .3-CD)PYRENE . Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
ISOPHORONE Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
2-METHYL-4,6-0INITROPHENOL Not detected ug/kg 2050 SW846-8270 21212000 15:21 HWC
I 2-METHYL NAPHTHALENE Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
2-METHYL-PHENOL Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
I 4-METHYL-PHENOL Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
NAPHTHALENE Not detected ug/kg 410 SW846-8270 2/212000 15:21 HWC
NITROBENZENE Not detected ug/kg 410 SW846-8270 2/212000 15:21 HWC
I 2-NITROPHENOL Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
4-NITROPHENOL Not detected ug/kg 2050 SW846-8270 21212000 15:21 HWC
N-NITROSOOIPHENYLAMINE Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
I N-NITROSODI-N-PROPYLAMINE Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
PENTACHLOROPHENOL Not detected ug/kg 2050 SW846-8270 21212000 15:21 HWC
I PHENANTHRENE Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
PHENOL Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
PYRENE Not detected ug/kg 410 SW846-8270 21212000 15:21 HWC
I NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
I .J,l'J ~pringbrooh. Hn.1d -. I'.<). Bo, 2-Hl:i-D-. Ch,1rlolll', ,"..;C 2.l-2::.--l-ll:i-D
l'hnnc: :-11v.;2Y-1i_-;11..i .... Toll hl'l' :\'umbL·1: \-Slltl/.;zy-6:;n-1 ..... F.n: "70-IAZ:i-n➔OY
I
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Lab Report
2/9/2000
Roy F. Weston, Inc
Ralph McKeen
5404 Metric Place
Norcross, GA 30092
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Lab Submittal Date/Time:
.: . ,M
;INC .
.. r-.'
Full Ser.iice Analy11ca1 & Environmental Solul1ons
Page 6 of 25
FCX-OU2-Remedial Action
FCW-9D L-A
AB56490
AO24F5
1/27/2000 10:55
1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST METHOD DATE/TIME
PARAMETER RESULT UNITS MDL REFERENCE STAIHED ANALYST
1,2,4-TRICHLOROBENZENE Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
2,4,5-TRICHLOROPHENOL Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
2.4,6-TRICHLOROPHENOL Not detected ug/kg 410 SW846-8270 2/2/2000 15:21 HWC
----------
Sample Comments:
Angela D. Overcash, V.P. boratory Services
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
I 1,1'1 Springbnmk lfo,1d ..-.. P.O. BP\ 2-lll;i.lJ-. Ch.Hlolh', ~C 2l-i22-1-03-J:.
l'hont·: 7!l~/S29-h.~b-l,.,. Toll fret' :'\urnbn: l-SOO/S2lJ-h.;b..J .-F.n: :-n..t/~25-ll-Hlq
------------·--------·----------------------------
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Lab Report
2/9/2000
Roy F. Weston, Inc
Ralph McKeen
5404 Metric Place
Norcross, GA 30092
Full Service Analytical & Environmenlal Solutions
Page 7 of 25
Customer Project ID: FCX-OU2-Remedial Action
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Lab Submittal Date/Time:
FCX-6L-A
AB56491
AO24F5
1/27/2000
1/27/2000
11:10
14:20
The following analytical resulls have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
METALS DIGESTION METHOD 3050
PREP. METHOD 3550
CHROMIUM. TOTAL
LEAD, TOTAL
C5-C8 Aliphatics
C9-C 12 Aliphatics
C9-C10 Aromatics
Surrogate% Recovery -PID
Surrogate% Recovery -FID
Dilution Factor
Ory Weight Received
EXTRACTION FOR EPH
C9-C 18 ALIPHATICS
C 19-C36 ALIPHATICS
C11-C22 AROMATICS
SURROGATE RECOVERY -ALIPHATIC
SURROGATE RECOVERY -AROMATIC
SURR:2-BROMONAPHTHALENE
SURR:2-FLUOROBIPHENYL
DILUTION FACTOR
DRY WEIGHT
CALCULATIONS BASED ON DRY WT.
BENZENE
BROMOBENZENE
SROMOCHLOROMETHANE
SROMODICHLOROMETHANE
SROMOFORM
SROMOMETHANE
TEST
RESULT
Completed
Completed
81
23
Not detected
Not detected
Not detected
76
87
13.41 g
Completed
Not detected
Not detected
Not detected
46
100
87
102
8.0 g
80
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
UNITS
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
%
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
%
%
%
mg/kg
mg/kg
% DRY WT.
ug/kg
ug/kg
uglkg
uglkg
ug/kg
ug/kg
MDL
1.0
METHOD
REFERENCE
3050
3550
6010
1.0 6010
7 MADEP VPH
6 MADEP VPH
2 MADEP VPH
(70-130) MADEP VPH
(70-130) MADEP VPH
MADEP VPH
MADEP VPH
40
MADEP-EPH
MADEP-EPH
20 MADEP-EPH
100 MADEP-EPH
(40-140) MADEP-EPH
(40-140) MADEP-EPH
(40-140) MADEP-EPH
(40-140) MADEP-EPH
0.01
6.0
6.0
6.0
6.0
6.0
12.0
MADEP-EPH
MADEP-EPH
SM 2540 G
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
DATErrlME
STARTED
21812000 08:00
112812000 08:00
21812000 16:11
21812000 16:11
112812000 23:02
112812000 23:02
112812000 23:02
112812000 23:02
112812000 23:02
112812000 23:02
112812000 23:02
ANALYST
GRR
JDP
MSP
MSP
KV
KV
KV
KV
KV
KV
KV
113112000 08:00 JDP
21412000 02: 11
21412000 02:11
21412000 02: 11
21412000 02: 11
21412000 02: 11
21412000 02: 11
21412000 02: 11
21412000 02: 11
21412000 02: 11
DMM
OMM
DMM
DMM
DMM
OMM
DMM
DMM
DMM
21112000 09:00 GAM
112712000 20:49 CMS
112712000 20:49 CMS
112712000 20:49 CMB
1127/2000 20:49 CMS
112712000 20:49 CMB
112712000 20:49 CMS
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
.1.1(1 Springb11H1"-H(),1J ..... l'.0. Bm J.rn_;.J:,..., Ch.ulo!!,', NC J,.;22.J-05,1:\
l'h11nl': :"ll-l/.=i24-lilh.t ..... Toll Fn'l' ~urnher: 1-snn1_;14-hJti•l .... r,1\: :-n.I,1_;2,;-n➔!lll
Lab Report
I Full Service Analy1icnl & Environmenlal Solulions
a 2/9/2000 Page 8 of 25
Roy F. Weston, Inc Customer Project ID: FCX-OU2-Remedial Action
Ralph McKeen Customer Sample ID: FCX-6L-A
D 5404 Metric Place Prism Sample ID: AB56491
Norcross, GA 30092 Login Group: AO24F5
Sample Collection Date/Time: 1/27/2000 11: 10
D Lab Submittal Date/Time: 1/27/2000 14 20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
I TEST TEST METHOD DATE/TIME
PARAMETER RESULT UNITS MDL REFERENCE STARTED ANALYST
I N-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/2712000 20:49 CMB
SEC-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260 1127/2000 20:49 CMB
TERT-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260 112712000 20:49 CMB
I CARBON TETRACHLORIDE Not detected ug/kg 6.0 SW846-8260 112712000 20:49 CMB
CHLOROBENZENE Not detected ug/kg 6.0 SW846-8260 1127/2000 20:49 CMB
CHLORODISROMOMETHANE Not detected ug/kg 6.0 SW846-8260 112712000 20:49 CMS
I CHLOROETHANE Not detected ug/kg 12.0 SW846-8260 112712000 20:49 CMB
CHLOROFORM Not detected ug/kg 6.0 SW846-8260 112712000 20:49 CMS
CHLOROMETHANE Not detected ug/kg 12.0 SW846-8260 112712000 20:49 CMB
I 2-CHLOROTOLUENE Not detected ug/kg 6.0 SW846-8260 112712000 20:49 CMB
4-CHLOROTOLUENE Not detected ug/kg 6.0 SW846-8260 112712000 20:49 CMS
I 1,2-DISROM0-3-CHLOROPROPANE Not detected ug/kg 12.0 SW846-8260 1127/2000 20:49 CMB
1,2-DIBROMOETHANE Not detected ug/kg 6.0 SW846-8260 112712000 20:49 CMB
DIBROMOMETHANE Not detected ug/kg 6.0 SW846-8260 112712000 20:49 CMB
I 1,2-DICHLOROSENZENE Not detected ug/kg 6.0 SW846-8260 112712000 20:49 CMB
1,3-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260 112712000 20:49 CMB
1.4-DICHLOROSENZENE Not detected ug/kg 6.0 SW846-8260 112712000 20:49 CMB
I DICHLORODIFLUOROMETHANE Not detected ug/kg 6.0 SW846-8260 112712000 20:49 CMB
1, 1-DICHLOROETHANE Not detected ug/kg 6.0 SW846-8260 1/2712000 20:49 CMB
I 1,2-DICHLOROETHANE Not detected ug/kg 6.0 SW846-8260 1127/2000 20:49 CMB
1, 1-DICHLOROETHENE Not detected ug/kg 6.0 SW846-8260 1127/2000 20:49 CMB
CIS-1,2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-8260 112712000 20:49 CMB
I TRANS-1,2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-8260 112712000 20:49 CMS
1,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260 1127/2000 20:49 CMS
1,3-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260 112712000 20:49 CMS
I 2,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:49 CMB
1, 1-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260 1/2712000 20:49 CMS
ETHYLSENZENE Not detected ug/kg 6.0 SW846-8260 112712000 20:49 CMB
I HEXACHLOROSUTADIENE Not detected ug/kg 6.0 SW846-8260 1127/2000 20:49 CMB
ISOPROPYLSENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 20:49 CMG
I NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
I •l•l'l Sprinfhronk Ho.id -. 1'.0. Bo, 2 llFIJ -. Ch.ulotll', :'C 2:,;2::.J-ll'.'-t.::
J'ho1u·: 7ll➔/524-i1;\h-l -. Toll Fn•e :\urnbcr: 1-8()(1/529-1,::i.ti-l-. F.1,: :-n-J/52~-ll-HllJ
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Lab Report
2/9/2000
Roy F. Weston, Inc
Ralph McKeen
5404 Metric Place
Norcross, GA 30092
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
~·{ ·M /!NC . .
Full Service Analytical & Environmental Solutions
Page 9 of 25
FCX-OU2-Remedial Action
FCX-6L-A
AB56491
AO24F5
1/27/2000 11:10
Lab Submittal Date/Time: 1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
P-ISOPROPYLTOLUENE
METHYLENE CHLORIDE
NAPHTHALENE
N-PROPYLBENZENE
STYRENE
1, 1, 1,2-TETRACHLOROETHANE
1.1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE
TOLUENE
1,2.3-TRICHLOROBENZENE
1,2.4-TRICHLOROBENZENE
1,1,1-TRICHLOROETHANE
1, 1,2-TRICHLOROETHANE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
1,2,3-TRICHLOROPROPANE
1,2.4-TRIMETHYLBENZENE
1.3,5-TRIMETHYLBENZENE
VINYL CHLORIDE
TOTAL XYLENES
2-BUTANONE (MEK)
2-CHLOROETHYL VINYL ETHER
4-METHYL-2-PENTANONE (MIBK)
ACETONE
CARBON DISULFIDE
VINYL ACETATE
CIS-1,3-DICHLOROPROPENE
TRANS-1,3-DICHLOROPROPENE
2-HEXANONE
IPE
TEST
RESULT
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
UNITS
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
MDL
6.0
120.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
12.0
6.0
60.0
12.0
60.0
120.0
120.0
60.0
6.0
6.0
60.0
6.0
METHOD
REFERENCE
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
DATEfTIME
STARTED ANALYST
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMS
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
1/2712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
1/2712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
112712000 20:49 CMB
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
.J.;4 Springbrook Ho.id .... 1'.U. Bo, 2-l05-l.1 .... Charlott,,, NC 2S2:.i-t-05-1.1
l'honl': :"ll-l/52tJ.h3h~ .... Tnll F1l'l' :-..:umbt>r: l-S0062'-l-fl:1h-l .... F,1,: -:0-1/525-n-lnq
I
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Lab Report
2/9/2000
Roy F. Weston, Inc
Ralph McKeen
5404 Metric Place
Norcross, GA 30092
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sam pie Collection Date/Time:
Lab Submittal Date/Time:
Full Service Analytical & Erwironmental Solutions
Page 10 of 25
FCX-OU2-Remedial Action
FCX-6L-A
AB56491
AO24F5
1/27/2000 11:10
1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
MTBE
SURR:DIBROMOFLUOROMETHANE
SURR:TOLUENE-D8
SURR:BROMOFLUOROBENZENE
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
BENZO(A)ANTHRACENE
BENZO(B)FLUORANTHENE
BENZO(K)FLUORANTHENE
BENZO(A)PYRENE
BENZO(GHI )PERY LENE
BIS(2-CHLOROETHOXY)METHANE
BIS(2-CHLOROETHYL)ETHER
BIS(2-CHLOROISOPROPYL)ETHER
BIS(2-ETHYLHEXYL)PHTHALATE
4-BROMOPHENYL PHENYL ETHER
BUTYL BENZYL PHTHALATE
4-CHLORO-3-METHYLPHENOL
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
4-CHLOROPHENYL PHENYL ETHER
CHRYSENE
DIBENZO(A.H)ANTHRACENE
DIBENZOFURAN
DI-N-BUTYLPHTHALATE
1,2-DICHLOROBENZENE
1.3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
TEST
RESULT
Not detected
93
90
82
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
UNITS
ug/kg
%
%
%
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
MDL
6.0
70-130
70-130
70-130
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
METHOD
REFERENCE
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SWB46-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
DATE/TIME
STARTED ANALYST
1127/2000 20:49 CMB
1127/2000 20:49 CMB
112712000 20:49 CMB
1127/2000 20:49 CMB
21212000 16:22
21212000 16:22
21212000 16:22
21212000 16:22
21212000 16:22
212/2000 16:22
21212000 16:22
21212000 16:22
21212000 16:22
21212000 16:22
21212000 16:22
21212000 16:22
21212000 16:22
21212000 16:22
21212000 16:22
21212000 16:22
21212000 16:22
21212000 16:22
21212000 16:22
21212000 16:22
21212000 16:22
21212000 16:22
21212000 16:22
21212000 16:22
21212000 16 22
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
I ➔-llJ Springhrool,. Ro.id -.1'.0. Bm '.:-l!lS-L~ -.Ch.1rloth•, ;\;C '.:S~:?A-0'.'-l.1
l'honl': 70-l/5~Y-h.1b..J -. Toll Fret' :'\'umber: l-/'l(lll/52Y-h.16..J .-1:.n: 70-l/32:'.-\l-lnG
---------------------------------------------------
-·• lab Report ' ... '
I M
S:'1Nc.
fi,,
I Full Servico Analytical & Environmental Solutions
B 2/9/2000 Page 11 of 25
Roy F. Weston, Inc Customer Project ID: FCX-OU2-Remedial Action
Ralph McKeen Customer Sample ID: FCX-6L-A u 5404 Metric Place Prism Sample ID: AB56491
Login Group: AO24F5 Norcross, GA 30092 Sample Collection Date/Time: 1/27/2000 11: 10
m Lab Submittal Date/Time: 1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
I TEST TEST METHOD DATE/TIME
PARAMETER RESULT UNITS MDL REFERENCE STARTED ANALYST
I 2,4-DICHLOROPHENOL Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
DIETHYL PHTHALATE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
2,4-DIMETHYLPHENOL Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
I DIMETHYL PHTHALATE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
2,4-DINITROPHENOL Not detected ug/kg 2050 SW846-8270 21212000 16:22 HWC
2,4-0INITROTOLUENE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
I 2,6-DINITROTOLUENE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
DI-N-OCTYLPHTHALATE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
I FLUORANTHENE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
FLUORENE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
HEXACHLOROBENZENE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
I HEXACHLOROBUTADIENE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
HEXACHLOROCYCLOPENTADIENE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
HEXACHLOROETHANE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
I INDENO(1,2,3-CD)PYRENE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
ISOPHORONE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
2-METHYL-4,6-DINITROPHENOL Not detected ug/kg 2050 SW846-8270 21212000 16:22 HWC
I 2-METHYL NAPHTHALENE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
2-METHYL-PHENOL Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
I 4-METHYL-PHENOL Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
NAPHTHALENE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
NITROBENZENE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
I 2-NITROPHENOL Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
4-NITROPHENOL Not detected ug/kg 2050 SW846-8270 21212000 16:22 HWC
N-NITROSODIPHENYLAMINE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC • N-NITROSODI-N-PROPYLAMINE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
PENTACHLOROPHENOL Not detected ug/kg 2050 SW846-8270 21212000 16:22 HWC
I PHENANTHRENE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
PHENOL Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
PYRENE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
I NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
I ·l..JIJ Springlnook H.n,1d -. l'.O. Bo, 2405-IJ .... Ch.1rlo1!{', NC 2822-l-llS-L~
l'hom·: 70..J/529-hJfd ..... Tull Frel' !\'umlwr: I-800/329-tiJh..J .... Ln: 70..J/:i25-0..J(1•l
I
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Lab Report
2/9/2000
Roy F. Weston, Inc
Ralph McKeen
5404 Metric Place
Norcross, GA 30092
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Full Service Analytical & Environmental Solutions
Page 12 of 25
FCX-OU2-Remedial Action
FCX-6L-A
AB56491
AO24F5
1/27/2000 11:10
Lab Submittal Date/Time: 1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST METHOD DATE/TIME
PARAMETER RESULT UNITS MDL REFERENCE STARTED ANALYST
1.2.4-TRICHLOROBENZENE Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
2,4,5-TRICHLOROPHENOL Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
2,4,6-TRICHLOROPHENOL Not detected ug/kg 410 SW846-8270 21212000 16:22 HWC
----------
Sample Comments:
Ange1~·6. Overcash, V.P. Laboratory Services
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
-l-19 Springbrook Ruad .... l'.O. Bo., 2-lllS-1.1-. Ch.Hlnlll', NC 2822-1-05-P l _____________ l'1_"_'"_•·_= _;,_,.,_1s_2_,, ___ "_''_'➔_-_·,_·.,_1 '_"_"_.,._,.,_· "_'_"_b,_· ,_: _,-_s,_10_1s_2_•1-_"_'"_➔_-_1_=.1_"_;_n_➔1_s_2s_.,_J➔_o_<J ____________ _
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Lab Report I !·
:·INC.
~}
Full Service Analy1ical & Env1ronmentnl Solutions
2/9/2000 Page 13 of 25
Roy F. Weston, Inc Customer Project ID: FCX-OU2-Remedial Action
Ralph McKeen Customer Sample ID: FCX-8DL-A
5404 Metric Place Prism Sample ID: AB56492
Norcross, GA 30092 Login Group: AO24F5
Sample Collection Date/Time: 1/27/2000 11 :35
Lab Submittal Date/Time: 1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST METHOD DATErrlME
PARAMETER RESULT UNITS MDL REFERENCE STARTED ANALYST
METALS DIGESTION METHOD 3050 Completed 3050 2/8/2000 08:00 GRR
PREP. METHOD 3550 Completed 3550 1/28/2000 08:00 JDP
CHROMIUM, TOTAL 82 mg/kg 1.0 6010 2/8/2000 16: 14 MSP
LEAD. TOTAL 20 mg/kg 1.0 6010 2/8/2000 16:14 MSP
CS-CB Aliphalics Not detected mg/kg 7 MADEP VPH 1/28/2000 23 56 KV
C9-C 12 Aliphatics Not detected mg/kg 6 MADEP VPH 1/28/2000 23:56 KV
C9-C 1 O Aromatics Not detected mg/kg 2 MADEP VPH 1/28/2000 23:56 KV
Surrogate% Recovery -PJD 74 % (70-130) MADEP VPH 1/28/2000 23:56 KV
Surrogate % Recovery -FID 79 % (70-130) MADEP VPH 1/28/2000 23:56 KV
Dilution Factor mg/kg MADEP VPH 1/28/2000 23:56 KV
Dry Weight Received 13.09 g mg/kg MADEP VPH 1/28/2000 23:56 KV
----------
EXTRACTION FOR EPH Completed MADEP-EPH 1 /3112000 08:00 JDP
C9-C18 ALIPHATICS Not detected mg/kg 40 MADEP-EPH 2/4/2000 03:02 DMM
C19-C36 ALIPHATICS Not detected mg/kg 20 MADEP-EPH 2/4/2000 03:02 DMM
C11-C22 AROMATICS Not detected mg/kg 100 MADEP-EPH 2/4/2000 03:02 DMM
SURROGATE RECOVERY· ALIPHATIC 53 % (40-140) MADEP-EPH 2/4/2000 03:02 DMM
SURROGATE RECOVERY· AROMATIC 111 % (40-140) MADEP-EPH 2/4/2000 03:02 DMM
SURR:2-BROMONAPHTHALENE 104 % (40-140) MADEP-EPH 2/4/2000 03:02 DMM
SURR:2-FLUOROBIPHENYL 106 % (40-140) MADEP-EPH 2/4/2000 03:02 DMM
DILUTION FACTOR mg/kg MADEP-EPH 2/4/2000 03:02 DMM
DRY WEIGHT 7.8 g mg/kg MADEP-EPH 2/4/2000 03:02 DMM
----------
CALCULATIONS BASED ON DRY WT. 78 % DRY WT. 0.01 SM 2540 G 2/1/2000 09:00 GAM
BENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 21:35 CMB
BROMOBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 21:35 CMB
BROMOCHLOROMETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 21:35 CMB
BROMODICHLOROMETHANE Not detected uglkg 6.0 SW846-8260 1/27/2000 21:35 CMB
BROMOFORM Not detected ug/kg 6.0 SW846-8260 1/27/2000 21:35 CMB
BROMOMETHANE Not detected uglkg 12.0 SW846-8260 1/27/2000 21:35 CMB
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
I
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Lab Report
2/9/2000
Roy F. Weston, Inc
Ralph McKeen
5404 Metric Place
Norcross, GA 30092
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Full Service Analytical & Env1ro11menlal Solutions
Page 14 of 25
FCX-OU2-Remedial Action
FCX-8D L-A
AB56492
AO24F5
1/27/2000 11 :35
Lab Submittal Date/Time: 1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
N-BUTYLBENZENE
SEC-BUTYLBENZENE
TERT-BUTYLBENZENE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLORODIBROMOMETHANE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
2-CHLOROTOLUENE
4-CHLOROTOLUENE
1.2-DIBROMO-3-CHLOROPROPANE
1.2-DIBROMOETHANE
DIBROMOMETHANE
1.2-DICHLOROBENZENE
1.3-DICHLOROBENZENE
1.4-DICHLOROBENZENE
DICHLORODIFLUOROMETHANE
1.1-DICHLOROETHANE
1,2-DICHLOROETHANE
1, 1-DICHLOROETHENE
CIS-1.2-DICHLOROETHENE
TRANS-1.2-DICHLOROETHENE
1.2-DICHLOROPROPANE
1.3-DICHLOROPROPANE
2,2-DICHLOROPROPANE
1, 1-DICHLOROPROPENE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
TEST
RESULT
Not detected
Not detected
Not detected
Not detected
Not detected
Nol detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
UNITS
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
MDL
6.0
6.0
6.0
6.0
6.0
6.0
12.0
6.0
12.0
6.0
6.0
12.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
METHOD
REFERENCE
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SWB46-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
DATE/TIME
STARTED ANALYST
1/27/2000 21:35 CMB
1/27/2000 21 :35 CMB
1/27/2000 21:35 CMB
1/27/2000 21:35 CMB
1/27/2000 21 :35 CMB
1/27/2000 21 :35 CMB
1/27/2000 21:35 CMB
1/27/2000 21:35 CMB
1127/2000 21:35 CMB
1/27/2000 21:35 CMB
1/27/2000 21:35 CMB
1/27/200021:35 CMB
1/27/2000 21:35 CMB
1/2712000 21:35 CMB
1/27/2000 21 :35 CMB
1127/2000 21:35 CMB
1/2712000 21:35 CMB
1/27/2000 21:35 CMB
1/27/2000 21:35 CMB
1/27/2000 21:35 CMB
1/27/200021:35 CMB
1/27/2000 21 :35 CMB
1/27/2000 21:35 CMB
1/27/2000 21:35 CMB
1/27/2000 21 :35 CMB
1/2712000 21:35 CMB
1/27/2000 21:35 CMB
1/27/2000 21:35 CMB
1/27/2000 21:35 CMB
1/27/2000 21:35 CMB
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Waler Cert. No. 37735 -FL Certification N. E87519
I, __ -1-l'l Springhnmk J{o,1d -P.()_ Bn, 2-1!15-J,1 -Ch.nlotte, ;\1C 21"''.!2--1-();;.J:;
!'hrnll': :-n--1;_;1•J-1'.1h--l ..-Tnll hct' 1-...:umbl'l' J-H00/529-f'o.~t,--I -F.1,: :-O--li:'2S-O-Hl4
Lab Report
I
I Full Service Analytic.ii & Environmental Solul1ons
I' 2/9/2000 Page 15 of 25
Roy F. Weston, Inc Customer Project ID: FCX-OU2-Remedial Action
Ralph McKeen Customer Sample ID: FCX-8DL-A
I 5404 Metric Place Prism Sample ID: AB56492
Norcross, GA 30092 Login Group: A024F5
Sample Collection Date/Time: 1/27/2000 11 :35
I Lab Submittal Date/Time: 1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
I TEST TEST METHOD DATErrlME
PARAMETER RESULT UNITS MDL REFERENCE STARTED ANALYST
I P-ISOPROPYLTOLUENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 21 :35 CMB
METHYLENE CHLORIDE Not detected ug/kg 120.0 SW846-8260 1/27/2000 21:35 CMB
NAPHTHALENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 21:35 CMB
I N-PROPYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 21:35 CMB
STYRENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 21:35 CMB
1.1.1.2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 21:35 CMB
I 1. 1.2.2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 21:35 CMB
TETRACHLOROETHENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 21:35 CMB
TOLUENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 21 :35 CMB
I 1,2,3-TRICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 21 :35 CMB
1,2,4-TRICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 21:35 CMB
I 1, 1, 1-TRICHLOROETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 21:35 CMB
1.1,2-TRICHLOROETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 21:35 CMB
TRICHLOROETHENE Not detected ug/kg 6.0 SW846-8260 1/27/20D0 21:35 CMB
I TRICHLOROFLUOROMETHANE Not detected ug/kg 6.0 SW846-8260 1/27/20D0 21:35 CMB
1,2,3-TRICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 21:35 CMB
1,2,4-TRIMETHYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/20D0 21:35 CMB
I 1,3,5-TRIMETHYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 21:35 CMB
VINYL CHLORIDE Not detected ug/kg 12.0 SW846-8260 1/27/20D0 21:35 CMB
I TOTAL XYLENES Not detected ug/kg 6.0 SW846-8260 1/27/2000 21:35 CMB
2-BUTANONE (MEK) Nol detected ug/kg 60.D SW846-8260 1/27/2000 21 :35 CMB
2-CHLOROETHYL VINYL ETHER Not detected ug/kg 12.0 SW846-826D 1/27/2000 21:35 CMB
I 4-METHYL-2-PENTANONE (MIBK) Not detected ug/kg 60.0 SW846-8260 1/27/2000 21 :35 CMB
ACETONE Not detected ug/kg 120.0 SW846-8260 1/27/2000 21:35 CMB
CARBON DISULFIDE Not detected ug/kg 120.0 SW846-826D 1/27/2000 21:35 CMB
I VINYL ACETATE Not detected ug/kg 60.0 SW846-8260 1/27/2000 21 :35 CMB
CIS-1,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-826D 1/27/2000 21:35 CMB
TRANS-1,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 21:35 CMB
I 2-HEXANONE Not detected ug/kg 60.0 SW846-8260 1/27/2000 21:35 CMB
IPE Not detected ug/kg 6.0 SW846-8260 1/27120D0 21:35 CMB
I NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
I ➔➔q ~prin,i_:b1m1h Hu,1d .-l'.O. Hm ~•lll5•l.1..., Ch.nlotte, ;\'.C 2822-1-tl:S•l.1,
l'hlllll''. :-O..J/:,24-h.1h..! .-Toll hl'\' :\umbt·r: J-SOlll'.'24-h~b..J ..-Ln: ';'(1.162:i-O•Hl{l
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Lab Report
2/9/2000
Roy F. Weston, Inc
Ralph McKeen
5404 Metric Place
Norcross, GA 30092
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Lab Submittal Date/Time:
1
'M
'. INC.
'
Full Service Analytic:11 & Environmentul Solutions
Page 16 of 25
FCX-OU2-Remedial Action
FCX-BDL-A
AB56492
AO24F5
1/27/2000 11:35
1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
MTBE
SURR:DIBROMOFLUOROMETHANE
SURR:TOLUENE-D8
SURR:BROMOFLUOROBENZENE
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
BENZO(A)ANTHRACENE
BENZO(B)FLUORANTHENE
BENZO(K)FLUORANTHENE
BENZO(A)PYRENE
BENZO(GHl)PERYLENE
BIS(2-CHLOROETHOXY)METHANE
BIS(2-CHLOROETHYL)ETHER
BIS(2-CHLOROISOPROPYL)ETHER
BIS(2-ETHYLHEXYL)PHTHALATE
4-BROMOPHENYL PHENYL ETHER
BUTYL BENZYL PHTHALATE
4-CHLORO-3-METHYLPHENOL
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
4-CHLOROPHENYL PHENYL ETHER
CHRYSENE
DIBENZO(A.H)ANTHRACENE
DIBENZOFURAN
DI-N-BUTYLPHTHALATE
1.2-DICHLOROBENZENE
1.3-DICHLOROBENZENE
1.4-DICHLOROBENZENE
TEST
RESULT
Not detected
94
97
92
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Nol detected
Not detected
Not detected
Not detected
UNITS
ug/kg
%
%
%
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
MDL
6.0
70-130
70-130
70-130
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
METHOD
REFERENCE
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
DATE/TIME
STARTED ANALYST
1/27/2000 21:35 CMB
1/27/2000 21:35 CMB
1/27/2000 21:35 CMB
1/27/2000 21:35 CMB
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
212/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
21212000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
.).J1J Springhrnnk l{P,1d-. l'.0. B1l\ :-.HJ5-Ll-. Ch.1il11tte. :".:C 2~:!21-0S.J'.1 I J'lwrw: :-n.J/.:.2lJ-h~h-l -. To 11 F ll't' !\'um l~l'L \-8(Hl/:i2lJ-ti::1,o..) -. L1,: ';"\l.J:'52:-•0.J(ll)
,______________ -------------------------~
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Lab Report
2/9/2000
Roy F. Weston, Inc
Ralph McKeen
5404 Metric Place
Norcross, GA 30092
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Full Service Analyhcal & Environmental Solutions
Page 17 of 25
FCX-OU2-Remedial Action
FCX-8DL-A
AB56492
AO24F5
1/27/2000 11 :35
Lab Submittal DatefTime: 1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
2.4-DICHLOROPHENOL
DIETHYL PHTHALATE
2.4-DIMETHYLPHENOL
DIMETHYL PHTHALATE
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2.6-DINITROTOLUENE
DI-N-OCTYLPHTHALATE
FLUORANTHENE
FLUORENE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROCYCLOPENTADIENE
HEXACHLOROETHANE
INDENO{1,2,3-CD)PYRENE
ISOPHORONE
2-METHYL-4,6-DINITROPHENOL
2-METHYL NAPHTHALENE
2-METHYL-PHENOL
4-METHYL-PHENOL
NAPHTHALENE
NITROBENZENE
2-NITROPHENOL
4-NITROPHENOL
N-NITROSODIPHENYLAMINE
N-NITROSODI-N-PROPYLAMINE
PENTACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRENE
TEST
RESULT
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
UNITS
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
MDL
420
420
420
420
2100
420
420
420
420
420
420
420
420
420
420
420
2100
420
420
420
420
420
420
2100
420
420
2100
420
420
420
METHOD
REFERENCE
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
DATE/TIME
STARTED ANALYST
2/2/2000 17:40 HWC
2/2/2000 17:40 HWC
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17 :4 0
2/2/2000 1740
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 17:40
2/2/2000 1740
2/2/2000 17:40
2/2/2000 17 :4 0
2/2/2000 17:40
2/2/2000 17:40
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 • FL Certification N. E87519
.J-t9 Sprin,1..;hniok Hoad ..... P.O. Bn, :rw:,.1,, ..... Ch.nlotle, 1\'C 2~22-t-05-Li
l'ho!ll': -;'(l.l/52•1-h~h.l ..... Tull ftl'l' \:umlwr: l-~(Hl/:i2ll-h::Hi-t...., Ln: ;04/:;:!:i-!1.l{)(l
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Lab Report
2/9/2000
Roy F. Weston, Inc
Ralph McKeen
5404 Metric Place
Norcross, GA 30092
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
FLJII Sorvice Analytical & Environmental Solutions
Page 18 of 25
FCX-OU2-Remedial Action
FCX-8DL-A
AB56492
AO24F5
1/27/2000 11:35
Lab Submittal Date/Time: 1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST METHOD DATErrlME
PARAMETER RESULT UNITS MDL REFERENCE STARTED ANALYST
1,2,4-TRICHLOROBENZENE Not detected ug/kg 420 SW846-8270 2/2/2000 1740 HWC
2,4,5-TRICHLOROPHENOL Not detected ug/kg 420 SW846-8270 2/2/2000 17:40 HWC
2,4,6-TRICHLOROPHENOL Not detected ug/kg 420 SW846-8270 2/2/2000 17:40 HWC
----------
Sample Comments:
I/
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
I -I.Pl Sprin~bmok H11,1d-. l'.0. BO\ 2../-0S-13 .... Ch.nloitl'. NC 2S22-Hl:si-D
, _____________ 1•_hnrll': ';"(l../-.'::i29-h.lh,l ..... Toll Fil'(' Numb_,•,_: _1-_s_111_11._:;2_"_-n_.,_b➔_-_1_:,1_,_: ;_11_.11_0_::::;_._"•_Jl_"_ -----------
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lab Report
2/9/2000
Roy F. Weston, Inc
Ralph McKeen
5404 Metric Place
Norcross, GA 30092
Full Service Analytical & Environmental Solutions
Page 19 of 25
Customer Project ID: FCX-OU2-Remedial Action
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
FCX-7GL-A
AB56493
AO24F5
1/27/2000 11 :45
Lab Submittal Date/Time: 1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
METALS DIGESTION METHOD 3050
PREP. METHOD 3550
CHROMIUM, TOTAL
LEAD.TOTAL
C5-C8 Aliphatics
C9-C 12 Aliphatics
C9-C 1 0 Aromatics
Surrogate% Recovery -PIO
Surrogate% Recovery -FID
Dilution Factor
Ory Weight Received
EXTRACTION FOR EPH
C9-C18 ALIPHATICS
C19-C36 ALIPHATICS
C 11-C22 AROMA TICS
SURROGATE RECOVERY· ALIPHATIC
SURROGATE RECOVERY· AROMATIC
SURR:2-BROMONAPHTHALENE
SURR:2-FLUOROBIPHENYL
DILUTION FACTOR
DRY WEIGHT
CALCULATIONS BASED ON DRY WT.
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
TEST
RESULT
Completed
Completed
86
22
· Not detected
Not detected
Not detected
74
78
12.46 g
Completed
Not detected
Not detected
Not detected
73
139
119
124
7.8 g
78
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
UNITS
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
%
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
%
%
%
mg/kg
mg/kg
% DRY WT.
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
MDL
1.0
METHOD
REFERENCE
3050
3550
6010
1.0 6010
7 MADEP VPH
6 MADEP VPH
2 MADEP VPH
(70-130) MADEP VPH
(70-130) MADEP VPH
MADEP VPH
MADEP VPH
40
MADEP-EPH
MADEP-EPH
20 MADEP-EPH
100 MADEP-EPH
(40-140) MADEP-EPH
(40-140) MADEP-EPH
(40-140) MADEP-EPH
(40-140) MADEP-EPH
0.0178
6.0
6.0
6.0
6.0
6.0
12.0
MADEP-EPH
MADEP-EPH
SM 2540 G
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8260
DATE/TIME
STARTED ANALYST
21812000 08:00 GRR
112812000 08:00 JDP
21812000 16:17
21812000 16:17
112912000 00:51
112912000 00:51
112912000 00:51
112912000 00:51
112912000 00:51
112912000 00:51
112912000 00:51
MSP
MSP
KV
KV
KV
KV
KV
KV
KV
113112000 08:00 JDP
21412000 03:54
21412000 03:54
21412000 03:54
21412000 03:54
21412000 03:54
21412000 03:54
21412000 03:54
21412000 03:54
21412000 03:54
DMM
DMM
DMM
DMM
DMM
DMM
DMM
DMM
DMM
21112000 09:00 GAM
112712000 22:20 CMB
112712000 22:20 CMB
112712000 22:20 CMB
112712000 22:20 CMB
112712000 22:20 CMB
112712000 22:20 CMS
NC Certification No. 402 • SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
-l..J'J Springhrnok J{o,1d -. l'.0. Bo, 2-105-1.1 -. Charlol!e, NC 2H2::!,l-05•B l _____________ ''_h_mh': 7(l.l/5::!Y-fl3h.t .... Toll Free :\'umhn: 1-800/524-6~6➔-. Ln: 70.t/525-!1•109
Lab Report -; ~ :,, . t:··'.
I M ·;1Nc. r
D Full Service Analytical & Environmental Solutions
I 2/9/2000 Page 20 of 25
Roy F. Weston, Inc Customer Project ID: FCX-OU2-Remedial Action
Ralph McKeen Customer Sample ID: FCX-7GL-A g 5404 Metric Place Prism Sample ID: AB56493
Norcross, GA 30092 Login Group: AO24F5
Sample Collection Date/Time: 1/27/2000 11 :45
u Lab Submittal Date/Time: 1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
D TEST TEST METHOD DATErrlME
PARAMETER RESULT UNITS MDL REFERENCE STARTED ANALYST
n N-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMB
SEC-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMB
TERT-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMB
0 CARBON TETRACHLORIDE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMB
CHLOROBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMB
CHLORODIBROMOMETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMB
D CHLOROETHANE Not detected ug/kg 12.0 SW846-8260 1/27/2000 22:20 CMB
CHLOROFORM Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
CHLOROMETHANE Not detected ug/kg 12.0 SW846-8260 1/27/2000 22:20 CMB u 2-CHLOROTOLUENE Nol detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
4-CHLOROTOLUENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMB
0 1,2-DIBROMO-3-CHLOROPROPANE Not detected ug/kg 12.0 SW846-8260 1/27/2000 22:20 CMS
1,2-DIBROMOETHANE Not detected ug/kg 6,0 SW846-8260 1/27/2000 22:20 CMB
DIBROMOMETHANE Not detected ug/kg 6,0 SW846-8260 1/27/2000 22:20 CMB
R 1,2-DICHLOROBENZENE Not detected ug/kg 6,0 SW846-8260 1/27/2000 22:20 CMB
1,3-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMB
1.4-DICHLOROBENZENE Not detected ug/kg 6,0 SW846-8260 1/27/2000 22:20 CMS u DICHLORODIFLUOROMETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMB
1, 1-DICHLOROETHANE Not detected ug/kg 6,0 SW846-8260 1/27/2000 22:20 CMB
u 1,2-DICHLOROETHANE Not detected ug/kg 6,0 SW846-8260 1/27/2000 22:20 CMS
1, 1-DICHLOROETHENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMB
CIS-1,2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMB
u TRANS-1,2-DICHLOROETHENE Not detected ug/kg 6,0 SW846-8260 1/27/2000 22:20 CMS
1,2-DICHLOROPROPANE Not detected ug/kg 6,0 SW846-8260 1/27/2000 22:20 CMB
1,3-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
D 2,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMB
1, 1-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
ETHYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMB
I HEXACHLOROBUTADIENE Not detected ug/kg 6,0 SW846-8260 1/27/2000 22:20 CMS
ISOPROPYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/2712000 22:20 CMS
u NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
I .j.Jq Springbrook Ho,1d .... P.O. Bo\ 2-105-n-.. Charlolll', NC 21i22-l-05-D
l'hrnll': :"0-1/52Y-b:H--.➔ .-Toll Fr('e Numbn: 1-800/529-h.lti.J .-F.l\: ";0-1625-0-l(lY
I
Lab Report
I Full Seivice Analytical & Environmen1a1 Solutions
m 2/9/2000 Page 21 of 25
Roy F. Weston, Inc Customer Project ID: FCX-OU2-Remedial Action
Ralph McKeen Customer Sample ID: FCX-7GL-A n 5404 Metric Place Prism Sample ID: AB56493
Login Group: AO24F5 Norcross, GA 30092 Sample Collection Date/Time: 1/27/2000 11 :45 u Lab Submittal Date/Time: 1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
H TEST TEST METHOD DATE/TIME
PARAMETER RESULT UNITS MDL REFERENCE STARTED ANALYST
D P-ISOPROPYLTOLUENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMB
METHYLENE CHLORIDE Not detected ug/kg 120.0 SW846-8260 1/27/2000 22:20 CMB
NAPHTHALENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMB
D N-PROPYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
STYRENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
1.1.1,2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
D 1, 1,2,2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
TETRACHLOROETHENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
TOLUENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
I 1,2,3-TRICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
1,2,4-TRICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
I 1.1.1-TRICHLOROETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
1, 1,2-TRICHLOROETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
TRICHLOROETHENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
m TRICHLOROFLUOROMETHANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
1,2.3-TRICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
1.2.4-TRIMETHYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
I 1,3,5-TRIMETHYLBENZENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
VINYL CHLORIDE Not detected ug/kg 12.0 SW846-8260 1/27/2000 22:20 CMS
I TOTAL XYLENES Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
2-BUTANONE (MEK) Not detected ug/kg 60.0 SW846-8260 1/27/2000 22:20 CMS
2-CHLOROETHYL VINYL ETHER Nol detected ug/kg 12.0 SW846-8260 1/27/2000 22:20 CMB
I 4-METHYL-2-PENTANONE (MIBK) Not detected ug/kg 60.0 SW846-8260 1/27/2000 22:20 CMS
ACETONE 420 ug/kg 120.0 SW846-8260 1/27/2000 22:20 CMS
CARBON DISULFIDE Not detected ug/kg 120.0 SW846-8260 1/27/2000 22:20 CMS
I VINYL ACETATE Not detected ug/kg 60.0 SW846-8260 1/27/2000 22:20 CMB
CIS-1,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMS
TRANS-1,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMB I 2-HEXANONE Not detected ug/kg 60.0 SW846-8260 1/27/2000 22:20 CMS
IPE Not detected ug/kg 6.0 SW846-8260 1/27/2000 22:20 CMB
I NC Certification No. 402 -SC Certification No. 99012 • NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
I .J.llJ Sprin~brools Hn,1d -. l'.U. Bo, 2--105➔3-. Charlotte, NC 2822..t-OS·D
l'lrnnv: -;'(l--I/529-b.1b.J-. Toll Fn'l' r\'urnbcr: l-t:HJ0/529-f,,1/l.J .... F.n: 70.J/.:;2:i-0.J(l4
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Lab Report
2/9/2000
Roy F. Weston, Inc
Ralph McKeen
5404 Metric Place
Norcross, GA 30092
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Full Service Ana!y1ical & Environmen1a1 Solutions
Page 22 of 25
FCX-OU2-Remedial Action
FCX-7GL-A
AB56493
AO24F5
1/27/2000 11:45
Lab Submiltal Date/Time: 1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
MTBE
SURR:DIBROMOFLUOROMETHANE
SURR:TOLUENE-D8
SURR:BROMOFLUOROBENZENE
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
BENZO(A)ANTHRACENE
BENZO(B)FLUORANTHENE
BENZO(K)FLUORANTHENE
BENZO(A)PYRENE
BENZO(GHl)PERYLENE
BIS(2-CHLOROETHOXY)METHANE
BIS(2-CHLOROETHYL)ETHER
BIS(2-CHLOROISOPROPYL)ETHER
BIS(2-ETHYLHEXYL)PHTHALATE
4-BROMOPHENYL PHENYL ETHER
BUTYL BENZYL PHTHALATE
4-CHLORO-3-METHYLPHENOL
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
4-CHLOROPHENYL PHENYL ETHER
CHRYSENE
DIBENZO(A.H)ANTHRACENE
DIBENZOFURAN
DI-N-BUTYLPHTHALATE
1 ,2-DICHLOROBENZENE
1 .3-DICHLOROBENZENE
1 .4-DICHLOROBENZENE
TEST
RESULT
Not detected
86
83
89
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
UNITS
ug/kg
%
%
%
uglkg
uglkg
ug/kg
ug/kg
ug/kg
uglkg
ug/kg
uglkg
uglkg
uglkg
uglkg
uglkg
uglkg
uglkg
uglkg
ug/kg
ug/kg
ug/kg
uglkg
uglkg
uglkg
uglkg
uglkg
uglkg
uglkg
MDL
6.0
70-130
70-130
70-130
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
METHOD
REFERENCE
SW846-8260
SW846-8260
SW846-8260
SW846-8260
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
SW846-8270
DATErflME
STARTED ANALYST
1/27/2000 22:20 CMB
1/27/2000 22:20 CMB
1/27/2000 22:20 CMB
1/27/2000 22:20 CMB
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
2/2/2000 18:27
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
HWC
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
I -1.Jl-l Springbrook l{oad-. P.O. Bn\ 2:.I0S-U-. Ch.irlolle, r-.:c 2H22.t-0S.l~
,,__ _____________ l'lwrll': -:-t)-1/S24-h.lh-l -. Toll Frt•P ~umber: I-H00/52lJ-h]h.t-. F,n: /().J/52:,-0-t!lll
• Lab Report
I Full Servico Analytical & Environmental Solutions
I 2/9/2000 Page 23 of 25
Roy F. Weston, Inc Customer Project ID: FCX-OU2-Remedial Action
Ralph McKeen Customer Sample ID: FCX-7GL-A g 5404 Metric Place Prism Sample ID: AB56493
Login Group: AO24F5 Norcross, GA 30092 Sample Collection Date/Time: 1/27/2000 11 :45
D Lab Submittal Date/Time: 1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
g TEST TEST METHOO DATE!TIME
PARAMETER RESULT UNITS MDL REFERENCE STARTED ANALYST
D 2.4-DICHLOROPHENOL Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
DIETHYL PHTHALATE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
2,4-DIMETHYLPHENOL Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
D DIMETHYL PHTHALATE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
2,4-DINITROPHENOL Not detected ug/kg 2100 SW846-8270 212/2000 18:27 HWC
2,4-DINITROTOLUENE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
I 2,6-DINITROTOLUENE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
DI-N-OCTYLPHTHALATE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
I FLUORANTHENE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
FLUORENE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
HEXACHLOROBENZENE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
I HEXACHLOROBUTADIENE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
HEXACHLOROCYCLOPENTADIENE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
HEXACHLOROETHANE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
I INDENO( 1,2,3-CD)PYRENE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
ISOPHORONE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
2-METHYL-4,6-DINITROPHENOL Not detected ug/kg 2100 SW846-8270 21212000 18:27 HWC
I 2-METHYL NAPHTHALENE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
2-METHYL-PHENOL Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
I 4-METHYL-PHENOL Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
NAPHTHALENE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
NITROBENZENE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
I 2-NITROPHENOL Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
4-NITROPHENOL Not detected ug/kg 2100 SW846-8270 21212000 18:27 HWC
N-NITROSODIPHENYLAMINE Nol detected ug/kg 420 SW846-8270 21212000 18:27 HWC
I N-NITROSODI-N-PROPYLAMINE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
PENTACHLOROPHENOL Not detected ug/kg 2100 SW846-8270 21212000 18:27 HWC
I PHENANTHRENE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
PHENOL Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
PYRENE Not detected ug/kg 420 SW846-8270 21212000 18:27 HWC
I NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
I ..J.Jq ~pringbro1lk Ho.id .-P.O. Bo\ 2•Hl5-U .-.. Ch.nlollt', NC 2822➔•05..J~
l'h(int': ';'0--1624-h31i•t-. Toll Frt't' ;-..;umbt·r: l-S00/524-fo3h-l _... F.1,: 70-l/525-ll-HN
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Lab Report
2/9/2000
Roy F. Weston, Inc
Ralph McKeen
5404 Metric Place
Norcross, GA 30092
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Lab Submittal Date/Time:
Full Service Analytical & Environmenlal Solutions
Page 24 of 25
FCX-OU2-Remedial Action
FCX-7GL-A
AB56493
A024F5
1/27/2000 11 :45
1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST METHOD DATErrlME
PARAMETER RESULT UNITS MDL REFERENCE STARTED ANALYST
1.2.4-TRICHLOROBENZENE Not detected ug/kg 420 SW846-8270 2/2/2000 18:27 HWC
2.4.5-TRICHLOROPHENOL Not detected ug/kg 420 SW846-8270 2/2/2000 18:27 HWC
2.4.6-TRICHLOROPHENOL Not detected ug/kg 420 SW846-8270 2/2/2000 18:27 HWC
----------
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
I 4-l 11 Sp1i11gbrnok Hu,1d ..... l'.0. Bm 2-l05..JJ ..... Ch.1rloilt•, NC 2822-f-0543
l'hrn1l': 70-1/524-h:Hd .-lo!! Frt'(' Number: I-H00/52'l-h36➔ ..... F.l\: 70..J/525-0409
----~-----~-----
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Lab Report
2/9/2000
Roy F. Weston, Inc
Ralph McKeen
5404 Metric Place
Norcross, GA 30092
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Full Sorvico Analytical & Environmontal Solutions
Page 25 of 25
FCX-OU2-Remedial Action
TRIP BLANK
AB56494
AO24F5
1/27/2000
Lab Submittal Date/Time: 1/27/2000 14:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST METHOD DATE/TIME
PARAMETER RESULT UNITS MDL REFERENCE STARTED ANALYST
C5-C8 Aliphatics Not detected mg/L 7 MADEP VPH 1/29/2000 01 :45 KV
C9-C 12 Aliphatics Not detected mg/L 6 MADEP VPH 1/29/2000 01 :45 KV
C9-C 1 O Aromatics Not detected mg/L 2 MADEP VPH 1/29/2000 01 :45 KV
Surrogate % Recovery -PIO 77 % (70-130) MADEP VPH 1/29/2000 01 :45 KV
Surrogate% Recovery -FID 92 % (70-130) MADEP VPH 1/29/2000 01 :45 KV
Dilution Factor mg/L MADEP VPH 1/29/2000 01 :45 KV
----------
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification N. E87519
I 1-!ll Sp1 ingbrook l{n.1d-. r.O. Ben. 2-105-IJ-. Ch.irloth>, NC 2t-22-J-05-l3
_____________ l'ho,w: :"O-l/5~1.J-h~/1..!-. Toll Fn't' :\'umber: 1-800/52g-h.1h➔-. F.n: 70.t/525-0-llll/
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k:\:00(d'-0:?5'-(,0.10,lJST.CLSK\FCX-SCR.J>OC 2,1 April 2000 Vcr~ion
APPENDIX C
CHAIN-OF-CUSTODY FORM
-
PrpJeet Name
CLIENT.
. SAMPLE DESCRIPTION ,-· . '
·-~~ ·;.;. -~ .. d 3 n!!'_(~
. DATE :f; .': COLL:ECTED
coLi.eCT'e·o : -MILITARY ff .S . 3 ;,Hq~R~:
NPOES,'. NC~=~ UST:
,sc·-~-'oriieR·_•_· _
-H--qaeUO!flOEl. !£El lRlll!J
PAQE4-0F ___ QUOTE ,_. -----------:',. ,c4.19;?lliingbfOOk;!loiid;:""'-;CIJarlotte,,N\: ?~217 ,., ,
;~. ,· 2-.::,P:O::Box 240543 ""':Charlotte, .NC-:28224°0543 . •
.. }rfoke_;]7%4~~29-~~-3:t4f•-\': F~~:'.704£5ir~0409. " ~;
,_ -=-·· t -
PRESS DOWN FIRMLY -3 COPIES
MATRIX
(S'ci1L,:
WATE'ROR
SLUBGEJ
. .
-~coNTAJN.Eiftj,PE CODES: A= Amber C = Clear G = Gtass P =.Pli3stlc;· . _:!L ~ r~·f_lon-Uned 9ap VOA ,,;_V~1aiile.Organics ·Ancli}'sis (ZerO Head Space)
REMARKS
SUB
LAB
CERT.
IDNO .
" OTHER: NC ___ _
SC __ ~_ OTHER __ ·_
SEE REVERSE FOR
TERMS & CONDITIONS
PRISM
LAB
IDNO.
.L
FINAL REPORT COPY
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PRISM
LABORATORIES, INC.
Full Service Analytical & Environmental Solutions
Main Office:
449 Springbrook Road
P.O. Box 240543
Charlotte, NC 28224-0543
Phone: [phone]
1 /800/529-6364
Fax: [phone]
The State of North Carolina requires the ,enclosed VPH and EPl-1 forms be submitted with
our laboratory report. Before submitting these forms to the state, please insert the project name
and/or site location.
Thank you.
Prism Laboratories, Inc.
Cc: Lab File
T:word/vphfonn/siteloca.doc
- - - --- - - - - ---!!!!I == ==i -.. liilil
VPH (Aliphatics/Aromatics) Laboratory Reporting Form Continued
Roy F. Weston, Inc. Laboratory Name Prism Laboratories, Inc. --'-----'----------------Client Name
Project Name
Site Location
_F_C_X_-_O_U_2_-_R_e_m_e_d_i a_l _A_c_t i_o _n _________ NC Certification # (Lab) _4.:..:0:..:2:.._ ___________ _
Statesv, I\ e /V L
J INCLUDE APPROPRIATE UNITS
... ,, .,. "-'''~~-,,, ,~~~-"'~i~ ,,-,,,.,~s•-,¼=F•r·d,~Wf" ... ~. ""f C•'"'"" • •✓-ai!'A"' •J, ·1 ¾•t .,. "'IIR'""'" . 'If" ':'-!!, 1,\¥'= ,,..-. ..,sr,,, .. ,~---<!-r:\'l!!•~"-;<";{.i'.~,:;.<:gi'.;: .,y .~;>;-:-,.;;~:. f4'1i',1 ;Jll'IS•:41,~ •. amp e, n or:ma ton,an · · .. ·na Yt tea• , eSU S'h•.;1; ,.;:$',:;,.'~,-4,'..:-,'r;~,~~• is,w•{l:l ";., .,._:,.~ ;::Y_~, !~~. :3,_ ;, --.,:1 •c,_s_, .• _,;.. ,,..-,_£..,_.,,~ -1.,5$,_,ti!i~ -""-' -.. ,...;.. ~--, =-,,,:•,•J':~_:.&,;q:,,1J!!'A""'~"'--. -,--..i,1,_ • .r,r;.;,,',-"·"·•· -,,;:.,,,,,,., ~ ;,,_,,~L -._.,_,-r;;:,·,r:~-'"-7i~•-"'''d!,'!i,,;[ , ;.v;J .<:-t.V -~ .!t .Ffk;;,,~,:-;.'\;:; ·_. __ ~. "t·""''C,1 "\\ :~1 C. .>
Sample Identification AB56490 AB56491 AB56492 AB56493 AB56494
Sample Matrix Soil Soil Soil Soil Trip Blank
Collection Option (for soil)* 1 1 1 1 N/A
Date Collected 1/27/2000 1/27/2000 1/27/2000 1/27/2000 N/A
Date Received 1/27/2000 1/27/2000 1/27/2000 1/27/2000 1/27/2000
Date Extracted 1/28/2000 1/28/2000 1/28/2000 1/28/2000 1/28/2000
Date Analyzed 1/28/2000 1/28/2000 1/28/2000 1/29/2000 1/29/2000
Dry Weight 12.79 g 1341 g 13.09 g 1246 g N/A
Dilution Factor 1 1 1 1 1
CS -CS Aliphatics** <7 mg/kg <7 mg/kg <7 mg/kg <7 mg/kg <7 mg/L
C9 -C12 Aliphatics** <6 mg/kg <6 mg/kg <6 mg/kg <6 mg/kg <6 mg/L
C9 -C10 Aromatics** <2 mg/kg <2 mg/kg <2 mg/kg <2 mg/kg <2 mg/L
Surrogate% Recovery -PIO 74% 76% 74% 74% 77%
Surrogate % Recovery -FID 86% 87% 79% 78% 92%
• Option 1 = Established fill line on vial Option 2 = Sampling Device (indicate brand, e.g. Encore) Option 3 = Field weight of soil
.. Unadjusted value. Should exclude the concentration of any surrogate(s). internal standards, and/or concentrations of other ranges that elute within the specified range.
~:•· fr'•S:E.G~-,;r·; 1-::::,t~ .-;;:·~v .?;.:; ~~~~~3~f~ ;;. . •9,s;;,.c:r "' 1q:~ic9~c12,;r;.,i r~ . .,~~~JJ } , ,~-.•-·",~~-,,:;:j, r,;c_;,~y~~•~,:...i:~
AB56490 AB56491 AB56492 AB56493 AB56494 rfl.ftf..l_1p!i_{lt"1ct:::1! tf~A1iih1t1C~~ ;":~;-~r~rn~t1c3~;1
Percent Recovery• Fortified Blank (Spike)• PID NA NA 95%
Relative Percent Difference -PIO Duplicate NA NA 7.0%
Percent Recovery -Fortified Blank (Spike) -FIO 106% 119% NA
Relative Percent Difference -FIO Duplicate 3.0% 4.0% NA
Page 1 Revision 5/6/98
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Page 2: Roy F. Weston
Proj: FCX-OU2-Remedial Action
VPH Laboratory Reporting Form
Initial Calibration Date 2/2/2000
Calibration Ranges and Limits
~i;..Tf'.''"~a nge~"'~ ;;.;•j;,"y_,';;!)111:),~~~i~'"" •11,1""'~"""~~ v,;ilj~~,:1tRl.!:if'.f,i;ifl':"f1 ~ •-.ffeXA,,.,. , """"'' ""'~ --¾]:11 ! ~ -~' -~-..,..,, .... ,1.... '5{, ·"· ,'.!. _.,,..-/" ...... _ .;;.,_;,.~------~~-·-•-·~·-· -Y>Ai> .... l.,
CS -CB Aliphatics 2.0 mg/kg 5.2 mg/kg 7.0 mg/kg
C9 -C12 Aliphatics 1.3 mg/kg 4.1 mg/kg 6.0 mg/kg
C9 -C10 Aromatics 04 mg/kg 1.3 mg/kg 2.0 mg/kg
NOTE: Please include units as appropriate
Met_hod ?f Quantitation (~ircle one) Curve o~~~
75 ug/L
C5 -CS 187.5 ug/L
Aliphatics 375 ug/L 12%
525 ug/L
C9 -C12
Aliphatics
C9-C10
Aromatics
750 ug/L
55 ug/L
137.5 ug/L
275 ug/L
385 ug/L
550 ug/L
10 ug/L
25 ug/L
50 ug/L
70 ug/L
100 ug/L
NOTE: Please indicate units as appropriate.
Calibration Check Date
Calibration Check
;!itt3s,tI!:~~.!19gf~
CS -CB Aliphatics
C9 -C12 Aliphatics
C9 -C10 Aromatics
MDL O Method Detection Limit
ML = Mimimum Limit
RL • Reportable Limit
1/28/2000
~'k"\1~l!evel,i,J~'l? 'I> .f.~-~1'-,,-,,~--,• . .--,._, ... ,J',. ,.,
375 ug/L
275 ug/L
50 ug/L
AB56490 AB56491 AB56492 AB56493 AB56494
2.0%
14%
~~-•c0,u.on1r~/if~ ~~~".,.,!,...-,;_~ . .:., J'M-.
10%
14%
7.0%
RPD • Relative Percent Difference
%RSD = Percent Relative Standard Deviation
CCC = Correlation Coefficient of Curve
Revision 5/6/98
-------------~~~---EPH (Aliphatics/Aromatics) Laboratory Reporting Form
Client Name Roy F. Weston, Inc.
Project Name: FCX-OU2-Remedial Action
Site Location Sf«tes0: / / e, . tJ C.
INCLUDE APPROPRIATE UNITS
Laboratory Name Prism Laboratories, Inc.
NC Certification# (Lab) _._40=2"-----------
tc't"'.1~t~'tft?,-W;'.t:~"j~,f~;'JSanf plejlnfor:m"atioff,ancll~nalyticalijRes~ulfs~~j;;ii.1.~l~4:,;:~;.t~i;.i•Jp~r~;illi"f1 .~_-'-:l2\. ¢, • '0o,,;s.~i:,.X . .,,,,,, , __ ,,_. •P•,·==-·""·•o-'"'" ~,, . ...,...~ ~-•-_,.,,,,_,..""i.,_..,_-,,.-. .;,-_ -·•-_. ~"""'.,·"·-•;~_-_P_,,.,,,.----~-·"'.,,C.;"'t~.M..'••·-.-,,'l _,.,:,,,,,-..;: ,.,,._ c.rov ... t!c'.'o-,··
Sample Identification AB56490 AB56491 AB56492 AB56493
Sample Matrix Soil Soil Soil Soil
Date Collected 1/27/2000 1/27/2000 1/27/2000 1/27/2000
Date Received 1/27/2000 1/27/2000 1/27/2000 1/27/2000
Date Extracted 1/31/2000 1/31/2000 1/31/2000 1/31/2000
Date Analyzed 2/4/2000 2/4/2000 2/4/2000 2/4/2000
Dry Weight 8.0 g 8.0 g 7.8 g 7.8 g
Dilution Factor 1 1 1 1
C9 -C18 Aliphatics* <40 mg/kg <40 mg/kg <40 mg/kg <40 mg/kg
C19 -C36 Aliphatics* <20 mg/kg <20 mg/kg <20 mg/kg <20 mg/kg
C11 -C22 Aromatics* <100 mg/kg <100 mg/kg <100 mg/kg <100 mg/kg
Surrogate% Recovery 53% 46% 53% 73%
Surrogate% Recovery 121% 100% 111% 139%
Fractionation Surrogate% Recovery 113% 87% 104% 119%
Fractionation Surrogate% Recovery 112% 102% 106% 124%
• Unadjusted value. Should exclude the concentration of any surrogate(s), internal standards, and/or concentrations of other ranges that elute within the specified range.
~~~,7~.""'4' -:z;_;:1 lli"c fg"JSc;j6T~ V , -.is, "tl'!·r~·z.•.; !1 ~,C9.-C18· .,, , .. cu ,,c22,.;
L~~~;£'i,,.. i'?:~"!~l ,H'_ •=•t-,,_..,;-"! *.➔~•;,t£·f'11?+ '.~ ~~;._,.,._., ~-i'~"'t'
AB56490 AB56491 AB56492 AB56493 ::t?'A~phatic~,:; t'/Alip_ha_tii:-1,,il r~10A'romatiC!i :4?,, -----• __ _. --
Percent Recovery -Fortified Blank (Spike) 51% 75% 95%
Relative Percent Difference -Sample Duplicates 20% 31% 25%
Page 1 Revision 5/6/98
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Page 2 Roy F. Weston
Proj. FCX-OU2-Remedial Action
Attachment 2
EPH Laboratory Reporting Form
Initial Calibration Date 1/29/2000
Calibration Ranges and Limits
.-./111!!1!:<a · eil1lil,i!l"J''l!Jli' --'r.,~·.1, ·,., ):"~9 •. it:'t:/ -~it; :t~~1~l'~ -.:C~i,:', zy,~11:,;1
C , • ._ ~-• (.\ !,. i?;i ;~t~:~r~7itl,~-~~-~;i,!/'t
C9 -C18 Aliphatics 10 mg/kg 32 mg/kg 40 mg/kg
C19 -C36 Aliphatics 5.7 mg/kg 18 mg/kg 20 mg/kg
C11 -C22 Aromatics 32 mg/kg 102 mg/kg 100 mg/kg
NOTE: Please include units as appropriate
Met_hod ~f Quantitation (circle one): Curve ~erage Response F~
60 mg/L
150 mg/L
C9-C18 300mg/L 15%
Aliphatics 450 mg/L
600 mg/L
C19 -C36
Aliphatics
C11-C22
Aromatics
1200 mg/L
80 mg/L
200 mg/L
400 mg/L
600 mg/L
800 mg/L
1600 mg/L
170 mg/L
425 mg/L
850 mg/L
1275 mg/L
1700 mg/L
3400 mg/L
NOTE: Please indicate units as appropriate.
Calibration Check Date
Calibration Check
•,l"~fflKange~"'fi'~ >t.i-·f .!, .: ;i: .~, -i~ "-·~, :il:...1.,'.:, ,..
C9 -C18 Aliphatics
C19 -C36 Aliphatics
C11 -C22 Aromatics
MDL= Method Detection Limit
ML= Minimum Limit
RL = Reportable Limit
2/3/2000
.. Ji\'1'1J.!!eV:el'~ffi!? ,. ; . : ..,_:.:;:,i_~.~--. • ,=]
300 mg/L
400 mg/L
850 mg/L
AB56490 AB56491 AB56492 AB56493
19%
16%
l'.!lf~""lll~Kt::l''"~tfW:"J,; .. ~.•-,_-_!,.,..~~-.:£rhi.!.!
11%
7.9%
3.0%
RPO= Relative Percent Difference
¾RSO = Percent Relative Standard Deviation
CCC = Correlation Coefficient of Curve
Revision 5/6/98