NCD095458527_19990319_FCX Inc. (Statesville)_FRBCERCLA RI_Pre-Design Investigation Report OU-3 - Volume 2 Appendix F Part 1-OCR

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PRE-DESIGN INVESTIGATION REPORT
FOR OPERABLE UNIT THREE (OU3)
FCX-STA TESVILLE SUPERFUND SITE,
STATESVILLE, NORTH CAROLINA
VOLUME 2
prepared for
El Paso Energy Corporation
1001 Louisiana Street
Houston, TX 77002
March 1999
27-60313.0()8
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APPENDIXF
ANALYTICAL LABO RA TORY REPORTS
F-1 Report for Preliminary VOC Analysis of Packer Test Samples
F-2 Reports for Natural Attenuation Parameters
F-3 Data Validation Report Dated August 24, 1998
F-4 Data Validation Report Dated January 29, 1999
F-5 Data Validation Reports Dated March 1, 1999
\ \TN\.SYS'\DATA '\PROJ\0313.08\PDI-CVR.DOC
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APPENDIX F-1
REPORT FOR PRELIMINARY voe
ANALYSIS OF PACKER TEST SAMPLES
\\TN\SYS\DATA\PROJ\0313.08\J'l)I-C\'RDOC
I Pace Analytical Services, Inc.
Aaa1¥tical
9800 Kincey Avenue, Suite 100
eace Huntersville, NC 28078
I Tel: [phone]
Fax: [phone]
DATE: 08/19/98
I PAGE: 3
Pace Project Number: 921135
Client Project ID: FCX Statesvull e
Sample No: 9272493 Date Co 11 ected: 08/18/98 Matrix: Water
lient Sample JD: W-20D 142' Date Received: 08/18/98
leters Results Units PRL Analyzed Analyst CftS# Footnotes
......................... -...... ·········· ········· . -........ . -..... -. -... ... -. ---.. . .........
'·· VOA
I/MS voes by 8260 Method: EPA 8260 Prep Method: EPA 8260
Dichlorodifluoromethane ND ug/L 10 08/18/98 VFT 75-71-8
• Chloromethane ND ug/L 10 08/18/98 VFT 74-87-3
Vinyl Chloride ND ug/L 10 08/18/98 VFT 75-01-4
IBromomethane ND ug/L 10 08/18/98 VFI 74-83-9
Chloroethane NO ug/L 10 08/18/98 VFT 75-00-3
Trichlorofluoromethane ND ug/L 10 08/18/98 VFT 75-69-4
1.1-Dichloroethene ND ug/L 5 08/18/98 VFT 75:35.4
f.ethylene Chloride ND ug/L 5 08/18/98 VFT 75-09-2
. trans-1.2-Dichloroethene ND ug/L 5 08/18/98 VFT 156-60-5
1,1-Dichloroethane ND ug/L 5 08/18/98 VFT 75-34-3
lis-1,2-Dichloroethene ND ug/L 5 08/18/98 VFT 156-59-2
.2-Dichloropropane ND ug/L 5 08/18/98 VFT 594-20-7
Chloroform 13 ug/L 5 08/18/98 VFT 67-66-3
aBromochloromethane ND ug/L 5 08/18/98 VFT 74-97-5
1,1.1-Trichloroethane ND ug/L 5 08/18/98 VFT 71-55-6
1,1-Dichloropropene ND ug/L 5 08/18/98 VFT 563-58-6
1,2-Dichloroethane ND ug/L 5 08/18/98 VFT 107-06-2
ICarbcn Tetrachloride ND ug/L 5 08/18/98 VFT 56-23-5
__ Benzene ND ug/L 5 08/18/98 VFT 71-43-2
Tri chl oroethene ND sg/L 5 08/18/98 VFT 79-01-6
.1.2-Dichloropropane ND ug/L 5 08/18/98 VFT 78-87-5
Dibromomethane ND ug/L 5 08/18/98 VFT 74-95-3
Bromodichloromethane ND ug/L 5 08/18/98 VFT 75-27-4
1 Toluene ND ug/L 5 08/18/98 VFT 108-88-3
1.1,2-Trichloroethane ND ug/L 5 08/18/98 VFT 79-00-5
· 1,3-Dichloropropane ND ug/L 5 08/18/98 VFT 142-28-9
_ Di bromochl oromethane ND ug/L 5 08/18/98 VFT 124-48-1 I Tetrach l oroethene 5,5 ug/L 5 08/18/98 VFT 127-18-4
1,2-Dibromoethane ND ug/L 5 08/18/98 VFT 106-93-4
Chlorobenzene ND ug/L 5 08/18/98 VFT 108-90-7
,1.1,1.2-Tetrachloroethane ND ug/L 5 08/18/98 VFT 630,-20-6
Ethyl benzene ND ug/L 5 08/18/98 VFT 100-41-4
m&p-Xylene ND ug/L 10 08/18/98 VFT 7816-60-0
. Styrene ND ug/L 5 08/18/98 VFT 100-42-5
1·0-Xylene (1,2-Dimethylbenzene) ND ug/L 5 08/18/98 VFT 95-47-6
8romoform ND ug/L 5 08/18/98 VFT 75-25-2
lboratory Certification IPs
C Wastewater 12
NC Drinking Water 37706 IC 99006
REPORT OF LABORATORY ANALYSIS
Laboratory Certification IDs
KY Drinking Water 90090
TN UST List
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
VA Drinking Water 213
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Pace Analytical
:elf elder
'.2 rench Landing Ori ve
:a,vi ll e, TN 37228
.,. Hr, Greg Christians
' .: [phone] x420
;o ·d results are reported on a dry weight basis
.. Sample No: 9272485
:lient Sample ID: W-20D 122'
•'eters Results Units
.... -..... -.. -................. -·········· .... -....
•t ·· VOA
GC/HS voes by 8260 Method: EPA 8260
•,i chl orodi fl uoromethane ND ug/L
hloromethane ND ug/L
Vinyl Chloride ND ug/L
~romomethane ND ug/L
hloroethane ND ug/L
richlorofluoromethane ND ug/L
.l,l·Dichloroethene ND ug/L
'Methylene Chloride ND ug/L
_.trans· 1, 2 ·Di chl oroethene ND ug/L
1.1-Dichloroethane ND ug/L
'is-1,2-Dichloroethene ND ug/L
,2-Dichloropropane ND ug/L
Chloroform 23 ug/L
.-Bromochl oromethane ND ug/L
.1. 1, 1-Trichl oroethane ND ug/L
l,l·Dichloropropene ND ug/L
1,2-Dichloroethane ND ug/L
, .....
• Carbon Tetrachloride ND ug/L
Benzene ND ug/L
' Trichloroethene ND ug/L
,.2-Dichloropropane ND ug/L
ibromomethane ND ug/L
Bromodichloromethane ND ug/L
.. Toluene ND ug/L
11,l,2-Trichloroethane ND ug/L
1,3-Dichloropropane ND ug/L
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: 704-875·9091
DA1E: 08/19/98
PAGE: 1
Pace Project Number: 921135
Client Project ID: FCX Statesvulle
Date Collected: 08/18/98 Matrix: Water
Date Received: 08/18/98
PRL Analyzed Analyst CAS# Footnotes
.. --...... ········ ·········· ··········
Prep Method: EPA 8260
10 08/18/98 VFT 75-71-8
10 08/18/98 VFT 74.37.3
10 08/18/98 VFT 75-01-4
10 08/18/98 VFT 74.33.9
10 08/18/98 VFT 75-00-3
10 08/18/98 VFT 75-69·4
5 08/18/98 VFT 75.35.4
5 08/18/98 VFT 75-09-2
5 08/18/98 VFT 156-60-5
5 08/18/98 VFT 75.34.3
5 08/18/98 VFT 156-59-2
5 08/18/98 VFT 594-20-7
5 08/18/98 VFT 67-66-3
5 08/18/98 VFT 74.97.5
5 08/18/98 VFT 71-55-6
5 08/18/98 VFT 563-58·6
5 08/18/98 VFT 107-06-2
5 08/18/98 VFT 56-23-5
5 08/18/98 VFT 71-43-2
5 08/18/98 VFT 79-01-6
5 08/18/98 VFT 78-87-5
5 08/18/98 VFT 74.95.3
5 08/18/98 VFT 75-27·4
5 08/18/98 VFT 108-88-3
5 08/18/98 VFT 79-00-5
5 08/18/98 VFT 142-28-9
'Qca!Qc.'. Qe~ificaliQ□ IQ~ L.aboral21:Y Qectifica1i2□ IQs
Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090 i Drinking Water 37706 TN UST List
99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.
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Pace Analytical
Sample No:
:lient Sample JD:
?lmeters
9272485
W-20D 122'
1--Dibromochloromethane
Tetrachloroethene
-1,2-Dibromoethane
Results
ND
ND
ND
Chlorobenzene ND 11.1.1.2-Tetrachloroethane ND
__ Ethyl benzene ND
__ m&p-Xylene ND
I Styrene ND
-a-Xylene (1.2-Dimethylbenzene) ND
Bromoform ND
11.1.2.2-Tetrachloroethane ND
Jsopropylbenzene (Cumene) ND
, 1.2.3-Trichloropropane ND
Bromobenzene ND
I n-Propylbenzene ND
' 2-Chlorotoluene ND
4-Chlorotoluene ND
11.3.5-Trimethylbenzene ND
.tert-Butylbenzene ND
1,2,4-Trimethylbenzene ND
. sec-Butylbenzene ND I 1,3-Dichlorobenzene ND
__ p-Jsopropyltoluene ND
1,4-Dichlorobenzene ND
11. 2 -Di ch 1 orobenzene ND
_ , n-Butyl benzene ND
1,2-Dibromo-3-Chloropropane ND I 1.2.4-Trichlorobenzene ND
Naphthalene ND
Hexachlorobutadiene ND
1,2,3-Trichlorobenzene ND I Dibromofluoromethane (S) 91
1.2-Dichloroethane-d4 (Sl 83
Toluene-dB (S) 96
, 4-Bromofluorobenzene (S) 105
I
~boratorv Certification lPs
Units
·········
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
X
X
X
X
Pace Analytical Services. Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
DATE: 08/19/98
PAGE: 2
Pace Project Number: 921135
Client Project ID: FCX Statesvulle
Date Collected: 08/18/98 Matrix: Water
Date Received: 08/18/98
PRL Analyzed Analyst CASI/ Footnotes
.......... . . . . . . -. .......... ...... -.. -
5 08/18/98 VFT 124-48-1
5 08/18/98 VFT 127-18-4
5 08/18/98 VFT 106-93-4
5 08/18/98 VFT 108-90-7
5 08/18/98 VFT 630-20-6
5 08/18/98 VFT 100-41-4
10 08/18/98 VFT 7816-60-0
5 08/18/98 VFT 100-42-5
5 08/18/98 VFT 95-47-6
5 08/18/98 VFT 75-25·2
5 08/18/98 VFT 79-34-5
5 08/18/98 VFT 98-82-8
5 08/18/98 VFT 96-18-4
5 08/18/98 VFT 108-86-1
5 08/18/98 VFT 103-65-1
5 08/18/98 VFT 95-49-8
5 08/18/98 VFT 106-43-4
5 08/18/98 VFT 108-67-8
5 08/18/98 VFT 98-06-6
5 08/18/98 VFT 95-63-6
5 08/18/98 VFT 135-98-8
5 08/18/98 VFT 541-73-1
5 08/18/98 VFT 99-87·6
5 08/18/98 VFT 106-46-7
5 08/18/98 VFT 95-50-1
5 08/18/98 VFT 104-51-8
5 08/18/98 VFT 96-12-8
5 08/18/98 VFT 120-82-1
5 08/18/98 VFT 91-20-3
5 08/18/98 VFT 87-68·3
5 08/18/98 VFT 87-61-6
08/18/98 VFT 1868-53-7
08/18/98 VFT 17060-07-0
08/18/98 VFT 2037-26-5
08/18/98 VFT 460-00-4
~C Wastewater 12 lg Drinking Water !;~~! REPORT OF LABORATORY ANALYSIS
Laboratory Certification IDs
KY Drinking Water 90090
TN UST List
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
VA Drinking Water 213
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Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
a Sample No: 9272493
W-20D 142' l ient Sample ID:
·aleters
1,1,2,2-Tetrachloroethane
sopropylbenzene (Cumene)
·· 1,2,3-Trichloropropane
lromobenzene
-Propylbenzene
-Chlorotoluene
4-Chlorotoluene
1,3,5-Trimethylbenzene
ert-Butylbenzene
· 1,2,4-Trimethylbenzene
-
ec-Butylbenzene
.3-0ichlorobenzene
-Isopropyltoluene
1,4-Dichlorobenzene ·.t · 2 · Di ch l orobenzene
-Butyl benzene
1,2-Dibromo-3-Chloropropane
-
.2.4-Trichlorobenzene
aphthalene
exachlorobutadiene
1,2,3-Trichlorobenzene
ibromofluoromethane (S)
.2-Dichloroethane-d4 (S)
Toluene-dB (S)
r•Bromofluorobenzene (SJ
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loratory Certification IDs
Wastewater 12
NC Drinking Water 37706 I 99006
Results Units
Date Collected:
Date Received:
Tel: [phone]
Fax: [phone]
DATE: 08/19/98
PAGE: 4
Pace Project Number: 921135
Client Project ID: FCX Statesvulle
08/18/98
08/18/98
Matrix: Water
PRL Analyzed Analyst CASII Footnotes
. --..... -. ......... -.. -...... . -... -. -...... -... . -........
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
94
89
100
105
ug/L 5 08/18/98 VFT 79-34-5
ug/L 5 08/18/98 VFT 98-82-8
ug/L 5 08/18/98 VFT 96-18-4
ug/L 5 08/18/98 VFT 108-86-1
ug/L 5 08/18/98 VFT 103-65-1
ug/L 5 08/18/98 VFT 95-49-8
ug/L 5 08/18/98 VFT 106-43-4
ug/L 5 08/18/98 VFT 108-67-8
ug/L 5 08/18/98 VFT 98-06-6
ug/L 5 08/18/98 VFT 95-63-6
ug/L 5 08/18/98 VFT 135-98-8
ug/L 5 08/18/98 VFT 541-73-1
ug/L 5 08/18/98 VFT 99-87-6
ug/L 5 08/18/98 VFT 106-46-7
ug/L 5 08/18/98 VFT 95-50-1
ug/L 5 08/18/98 VFT 104-51-8
ug/L 5 08/18/98 VFT 96-12·8
ug/L 5 08/18/98 VFT 120-82-1
ug/L 5 08/18/98 VFT 91-20-3
ug/L 5 08/18/98 VFT 87-68-3
ug/L 5 08/18/98 VFT 87-61·6
X 08/18/98 VFT 1868-53-7
X 08/18/98 VFT 17060-07·0
X 08/18/98 VFT 2037-26-5
X 08/18/98 VFT 460-00-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Laboratory Certification IDs
KY Drinking Water 90090
TN UST List
VA Drinking Water 213
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Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
,lmR FOOTNOTES
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Not Detected
Not Calculable
Pace Reporting Limit
Surrogate
H.boratorv Certification IDs \le Wastewater 12
1 Drinking Water :;~~:
Tel: [phone]
Fax: [phone]
DATE: 08/19/98
PAGE: 5
Pace Project Number: 921135
Client Project ID: FCX Statesvulle
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Laboratory Certification IDs
KY Drinking Water 90090
TN UST List
VA Drinking Water 213
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J-value table
Project: 921135
Eckenfelder
Sample#
9272485
. 9272493
Bromodichloromethane
Naphthalene
Acrylonitrile
Bromodichloromethane
Naphthalene
3.77ug/L
3.35ug/L
8.59ug/L
2.22ug/L
l.92ug/L
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Pace Analytical
Pace Analy1ical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: 704·875·9092
Fax: 704·875·9091
:c.lfelder
·2~rench Landing Ori ve
la,ille, TN 37228
.t. Hr. Greg Christians
'h : [phone] x420
1Cltch ID: 1825
.n sis Method: EPA 8260
,s i ated Pace Samples:
IEID BLANK: 9273467
\sSOciated Pace Samples:
I
:;i~:~~; ~; ~~~~~~~~~~~ ...... .
:hloromethane
iii Chloride
Ir methane
:h oroethane
r1· l orofl uoromethane
., ichloroethene
le lene Chloride
:rans-1.2-Dichloroethene . ,1i chloroethane
:i ,2·Dichloroethene
~. 2-Di chl oropropane
;~~~~:□methane
.•.~. Trichloroethane
, . l · Di chl oropropene
.,IJoichloroethane
:alJon Tetrachloride
lenzene
·rtfhloroethene
L ,IJ)i chl oropropane
}i bromomethane
llodichloromethane
ene
l, , · Trichloroethane
lboratorv Certification IDs
C Wastewater 12
NC Drinking Water 37706 I 99006
QUALITY COITTROL DATA DATE: 08/19/98
PAGE: 6
Pace Project Number: 921135
Client Project ID: FCX Statesvulle
QC Batch Method: EPA 8260
Analysis Description: GC/MS voes by 8260
9272485 9272493
9272485 9272493
Method
Blank
Units Result PRL Footnotes
········•· . - - -. . . . . . .......... ..........
ug/L ND 10
ug/L ND 10
ug/L ND 10
ug/L ND 10
ug/L ND 10
ug/L ND 10
ug/L ND 5
ug/L ND 5
ug/L ND 5
ug/L ND 5
ug/L ND 5
ug/L ND 5
ug/L ND 5
ug/L ND 5
ug/L ND 5
ug/L ND 5
ug/L ND 5
ug/L ND 5
ug/L ND 5
ug/L ND 5
ug/L ND 5
ug/L ND 5
ug/L ND 5
ug/L ND 5
ug/L ND 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Laboratory Certification IDs
KY Drinking Water 90090
TN UST List
VA Drinking Water 213
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Pace Analytical
I IETHOD BLANK: 9273467
\s,ciated Pace Samples:
:t~:e~-... ---------··· .....
'., 3-Di chl oropropane
i,· · omochloromethane
; achloroethene
~, • Di bromoethane
:h 1 orobenzene ,11, 2-Tetrachl oroethane
~ , ~ l benzene
l&p-Xyl ene :lene , lene (1.2-Dimethylbenzene)
!romoforrn
.,1--2,2-Tetrachloroethane
: ropylbenzene (Cumene)
~-,3-Trichloropropane
lromobenzene
, ,opyl benzene
'. l orate l uene
:-Chl oroto 1 uene
.,5-Trimethylbenzene
: -Butyl benzene
.. ,4-Trimethylbenzene
:ec-Butyl benzene
.• Dichlorobenzene
, opropyltoluene
.. 4-0ichlorobenzene
'. 'Di chl orobenzene
1 ty 1 benzene
.. -Dibromo-3-Chloropropane
,,4-Trichl orobenzene
l thalene
I chlorobutadiene
·_, 2, 3-Tri chl orobenzene
,,omofluoromethane (SJ
, Dichloroethane-d4 (SJ
."oluene-d8 (SJ
-,omofluorobenzene (S)
lboratory Certification 10s
92724B5
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
X
X
X
X
QUALITY CONTROL DATA
9272493
Method
Blank
Result PRL
.......... . .........
NO 5
ND 5
ND 5
ND 5
ND 5
ND 5
ND 5
ND 10
ND 5
ND 5
NO 5
ND 5
ND 5
ND 5
ND 5
ND 5
ND 5
ND 5
ND 5
ND 5
ND 5
ND 5
ND 5
ND 5
ND 5
ND 5
ND 5
ND 5
ND 5
ND 5
ND 5
ND 5
89
99
108
109
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
DATE: 08/19/98
PAGE: 7
Pace Project Number: 921135
Client Project ID: FCX Statesvulle
Footnotes
··········
NC Wastewater 12
NC Drinking Water 37706 f 99D06
REPORT OF LABORATORY ANALYSIS
Laboratory Certification IDs
KY Drinking Water 90090
TN UST List •
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. Inc.
VA Drinking Water 213
I
Pace Analytical
I
I
JRATORY CONTROL SAMPLE: 9273475
?teter Units
. . ... -. -......... -...... -.. ..........
Dichlorodifluoromethane ug/L
:lromethane ug/L
V l Chloride ug/L
3romomethane ug/L
,:,roethane ug/L
r hlorofluoromethane ug/L
l, Dichloroethene ug/L
➔ethylene Chloride ug/L
tts·l,2·Dichloroethene ug/L
I Dichloroethane ug/L
:i s-1. 2-Di chl oroethene ug/L
21Dichloropropane ug/L
·: roform ug/L
3 ochloromethane ug/L
l,l,l•Trichloroethane ug/L
IIDichloropropene ug/L
I Dichloroethane ug/L
:arbon Tetrachloride ug/L
3,ene ug/L
r hloroethene ug/L
l, -Dichloropropane ug/L
Jlmomethane ug/L
: dichloromethane ug/L
1 ene ug/L
l,1.2-Trichloroethane ug/L
llDichloropropane ug/L
J· omochlorornethane ug/L
retrachloroethene ug/L
l-Dibromoethane ug/L
: robenzene ug/L
l. ,1,2-Tetrachloroethane ug/L
:thylbenzene ug/L
~nXylene ug/L
) ene ug/L
,-Xylene (1,2-Dimethylbenzene) ug/L
llloform ug/L
l 2,2-Tetrachloroethane ug/L
lsopropylbenzene (Cumene) ug/L
l-3-Trichloropropane ug/L
i obenzene ug/L
1 opylbenzene ug/L
QUALITY CONTROL DATA
Spike LCS Spike
Cone. Result X Rec
. .........
50 49.78 99.6
50 43.35 86.7
50 42.32 84.6
50 51.55 103
50 41.69 83.4
50 56.32 113
50 49.84 99.7
50 52.23 104
50 49.41 98.8
50 45.36 90.7
50 45.77 91.5
50 57.84 116
50 51.66 103
50 57.43 115
50 51.94 104
50 50.85 102
50 48.05 96.1
50 65.10 130
50 48.81 97.6
50 53.07 106
50 48.13 96.3
50 53.83 108
50 50.70 101
50 54.02 108
50 49.42 98.8
50 46.92 93.8
50 51.90 104
50 54.99 110
50 51.11 102
50 49.87 99.7
50 53.70 107
50 47.78 95.6
100 95.32 95.3
50 51.24 102
50 48.03 96.1
50 52.59 105
50 44.03 88.1
50 50.90 102
50 48.04 96.1
50 46.00 92.0
50 45.57 91.1
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
DATE: 08/19/98
PAGE: 8
Pace Project Number: 921135
Client Project ID: FCX Statesvulle
Footnotes
. .........
lboratorv Certification IDs
C Wastewater 12 i Drinking Water !;~~: REPORT OF LABORATORY ANALYSIS
Laboratory Certification IDs
KY Drinking Water 90090
TN UST list
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. Inc.
VA Drinking Water 213
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Pace Analytical
,
LTORY CONTROL SAMPLE: 9273475
'atter . . . . -.. ---..................
'-Chl oroto 1 uene
:-,orotoluene
, . -Trimethylbenzene
:ert-Butylbenzene \If Tri methyl benzene
; Butyl benzene
, . i chl orobenzene
,-Isopropyltoluene
' .,Di chl orobenzene
'.. Di chl orobenzene
1-Butyl benzene
.. Ii bromo-3 -Chl oropropane
,_. -Tri chl orobenzene
la thalene
lexachl orobutadi ene . ·t · Tri chl orobenzene
Ii mofluoromethane (S)
'.2-Dichloroethane·d4 (S)
·,ene-d8 (S)
;. omofluorobenzene
I
m
0
m
I
I
CS)
Units
········••
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
QUALITY CONTROL DATA
Spike LCS Spike
Cone. Result X Rec
....... ..........
50 45.90 91.8
50 44.38 88.8
50 47.46 94.9
50 47.53 95.1
50 46. 72 93.4
50 45. 70 91.4
50 49.04 98.1
50 47.53 95.1
50 48.42 96.8
50 47.37 94.7
50 45.52 91.0
50 39.21 78.4
50 51.57 103
50 40.31 80.6
50 53.91 108
50 48.57 97.1
100
100
104
110
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
DATE: 08/19/98
PAGE: 9
Pace Project Number: 921135
Client Project ID: FCX Statesvulle
Footnotes
--. -.. -. -.
lboratory Certification IDs
C Wastewater 12 i Drinking Water !;~~: REPORT OF LABORATORY ANALYSIS
Laboratory Certification IDs
KY Drinking Water 90090
TN UST List
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, lnc.
VA Drinking Water 213
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Pace Analytical
)UITY CONTROL DATA PARAMETER FOOTNOTES
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
DATE: 08/19/98
PAGE: 10
Pace Project Number: 921135
Client Project ID: FCX Statesvulle
:o,stent with EPA guidelines unrounded concentrations
ID Not Detected
are displayed and have been used to calculate X Rec and RPO values.
IC Not Calculable 'RI :P
Pace Reporting Limit
Relative Percent Difference
:s)
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Surrogate
lboratorv Certification IDs
NC Wastewater 12
NC Drinking Water 37706 I 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Laboratory Certification 10s
KY Drinking Water 90090
TN UST List
VA Drinking Water 213
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APPENDIX F-2
REPORTS FOR
NATURAL ATTENUATION PARAMETERS
\ \ TN'5YS \DAT A \PROJ'\0313. 08 \J'DJ .CVR. DOC
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 04/30/98
DATE RECEIVED· 05/01/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING USEPA
ANALYTES LIMITS METHOD
Ammonia Nitrogen (non distilled) 0.10 350.3
Chloride 1.0 9251/325.2
Nitrate+Nitrite Nitrogen 0.10 353.2
Phosphorus, total 0.020 365.2
Sulfate 1.0 9038/375.4
TKN 2.0 351.2
TOC (NPOC) 1.0 415.1/9060
Total Alkalinity as CaCO3 1.0 310.1
VOA, Fatty Acids (9) 1.5 556oc··
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
227 French Landing Drive
Nashville, Tennessee 37228
615.255.2288
FAX [phone]
98002991
W-12s
04/30/98
UNITS CONC
mg/L u
mg/L 1.9
mg/L 1.7
mg/L u
mg/L 5.8
mg/L u
mg/L u
mg/L u
mg/L 5.7
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 04/30/98
DATE RECEIVED: 05/01/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.10
Phosphorus, total 0.020
Sulfate 1.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
556oc··
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98002992
W-12i
04/30/98
UNITS CONC
mg/L u
mg/L 30
mg/L 2.7
mg/L 0.027
mg/L 38
mg/L u
mg/L 1.3
mg/L 25
mg/L 34
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 04/30/98
DATE RECEIVED· 05/01/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.10
Phosphorus, total 0.020
Sulfate 1.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
556oc··
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98002993
W-18s
04/30/98
UNITS CONC
mg/L u
mg/L u
mg/L 0.43
mg/L 0.088
mg/L u
mg/L u
mg/L u
mg/L u
mg/L 23
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 04/30/98
DATE RECEIVED: 05/01/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.10
Phosphorus, total 0.020
Sulfate 2.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
5560C ..
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98002994
W-30i
04/30/98
UNITS CONC
mg/L 1.2
mg/L 30
mg/L u
mg/L 0.078
mg/L 35
mg/L u
mg/L 14
mg/L 170
mg/L 49
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 04/30/98
DATE RECEIVED: 05/01/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.10
Phosphorus, total 0.020
Sulfate 1.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
5560C ..
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98002995
W-10i
04/30/98
UNITS CONC
mg/L u
mg/L u
mg/L u
mg/L 0.022
mg/L 4.3
mg/L u
mg/L u
mg/L 38
mg/L 12
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 05/01/98
DATE RECEIVED: 05/01/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride · 1.0
Nitrate+Nitrite Nitrogen 0.10
Phosphorus, total 0.020
Sulfate 1.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
5560C**
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98002996
W-22s
05/01/98
UNITS CONC
mg/L u
mg/L 9.9
mg/L 9.5
mg/L u
mg/L 1.3
mg/L u
mg/L u
mg/L u
mg/L 14
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 04/29/98
DATE RECEIVED: 05/01/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.10
Phosphorus, total 0.020
Sulfate 1.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
556oc··
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98002997
W-20i
04/29/98
UNITS CONC
mg/L u
mg/L 14
mg/L 0.32
mg/L u
mg/L 6.8
mg/L u
mg/L u
mg/L 56
mg/L 26
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 04/29/98
DATE RECEIVED· 05/01/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.10
Phosphorus, total 0.020
Sulfate 1.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
5560C*
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98002998
W-20s
04/29/98
UNITS CONC
mg/L u
mg/L u
mg/L u
mg/L 0.045
mg/L u
mg/L u
mg/L u
mg/L 28
mg/L 12
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 04/29/98
DATE RECEIVED: 05/01/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.020
Phosphorus, total 0.020
Sulfate 1.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
5560C ..
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98002999
FB42998
04/29/98
UNITS CONC
mg/L u
mg/L u
mg/L u
mg/L u
mg/L u
mg/L u
mg/L u
mg/L u
mg/L 2.9
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 04/30/98
DATE RECEIVED· 05/01/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.10
Phosphorus, total 0.020
Sulfate 1.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaC03 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
5560C ..
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98003001
W-5s
04/30/98
UNITS CONC
mg/L u
mg/L 34
mg/L 1.2
mg/L u
mg/L u
mg/L u
mg/L 9.4
mg/L u
mg/L 12
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 05/01/98
DATE RECEIVED· 05/01/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.10
Phosphorus, total 0.020
Sulfate 10
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
5560C**
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98003002
W-24s
05/01/98
UNITS CONC
.
mg/L u
mg/L 14
mg/L 0.25
mg/L 0.12
mg/L 18
mg/L u
mg/L 1.3
mg/L 15
mg/L 17
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D
Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 04/29/98
DATE RECEIVED: 05/01/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.10
Phosphorus, total 0.020
Sulfate 1.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
556oc··
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98003003
W-20s Dupe
04/29/98
UNITS CONC
mg/L u
mg/L u
mg/L u
mg/L 0.069
mg/L u
mg/L u
mg/L u
mg/L 29
mg/L 2.9
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a
Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 04/29/98
DATE RECEIVED: 05/01/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.020
Phosphorus, total 0.020
Sulfate 1.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
5560C ..
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98003004
EB42998
04/29/98
UNITS CONC
mg/L 0.44
mg/L u
mg/L u
mg/L u
mg/L u
mg/L u
mg/L u
mg/L u
mg/L 2.9
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D
Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 05/01/98
DATE RECEIVED· 05/01/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.10
Phosphorus, total 0.020
Sulfate 1.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
5560C**
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98003005
W-22i
05/01/98
UNITS CONC
mg/L u
mg/L 16
mg/L 4.2
mg/L u
mg/L u
mg/L u
mg/L 1.0
mg/L 49
mg/L 34
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 05/01/98
DATE RECEIVED: 05/01/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.20
Phosphorus, total 0.020
Sulfate 1.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
5560C ..
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98003006
W-29i
05/01/98
UNITS CONC
mg/L u
mg/L 23
rrig/L 8.5
mg/L u
mg/L u
mg/L u
mg/L u
mg/L 8.1
mg/L 17
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 05/05/98
DATE RECEIVED: 05/07/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.10
Phosphorus, total 0.020
Sulfate 1.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
5560C**
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98003118
W-9s
05/05/98
UNITS CONC
mg/L u
mg/L 4.9
mg/L 1.3
mg/L 0.050
mg/L u
mg/L u
mg/L u
mg/L u
mg/L 5.7
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 05/05/98
DATE RECEIVED: 05/07/98
ECKENFELDER SAMPLE NUMBER
.
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.10
Phosphorus, total 0.020
Sulfate 1.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
5560C ..
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98003119
W-9s Dupe
05/05/98
UNITS CONC
mg/L u
mg/L 4.7
mg/L 1.3
mg/L 0.050
mg/L u
mg/L u
mg/L 1.0
mg/L u
mg/L 4.6
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1-
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m
fl
m
I
Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 05/05/98
DATE RECEIVED· 05/07/98
ECKENFELDE~ SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.10
Phosphorus, total 0.020
Sulfate 2.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351._2
415.1/9060
310.1
556oc··
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98003121
W-28i
05/05/98
UNITS CONC
mg/L u
mg/L 5.2
mg/L 0.14
mg/L 0.13
mg/L 42
mg/L u
mg/L 6.0
mg/L 84
mg/L 40
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I
Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 05/05/98
DATE RECEIVED: 05/07/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.10
Phosphorus, total 0.020
Sulfate 2.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
92511325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
5560C ..
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98003122
W-19s
05/05/98
UNITS CONC
mg/L u
mg/L 31
mg/L 0.45
mg/L 0.031
mg/L 47
mg/L u
mg/L u
mg/L 26
mg/L 18
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 05/05/98
DATE RECEIVED· 05/07/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.10
Phosphorus, total 0.020
Sulfate 1.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353'.2
365.2
9038/375.4
351.2
415.1/9060
310.1
5560C**
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98003123
W-5i
05/05/98
UNITS CONC
mg/L u
mg/L 2.0
mg/L u
mg/L 0.11
mg/L 22
mg/L u
mg/L 1.0
mg/L 39
mg/L 14
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 05/05/98
DATE RECEIVED· 05/07/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.40
Phosphorus, total 0.020
Sulfate 1.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
5560C ..
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98003126
W-17s
05/05/98
UNITS CONC
mg/L u
mg/L 27
mg/L 24
mg/L 0.041
mg/L u
mg/L u
mg/L 1.9
mg/L u
mg/L 5.7
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 05/05/98
DATE RECEIVED: 05/07/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.020
Phosphorus, total 0.020
Sulfate 1.0
TKN 2.0
TOG (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
5560C ..
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
98003127
FB5598
05/05/98
UNITS CONG
mg/L u
mg/L u
mg/L u
mg/L u
mg/L u
mg/L u
mg/L u
mg/L u
mg/L 2.9
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D
Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #0313
DATE SAMPLED: 05/05/98
DATE RECEIVED· 05/07/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
REPORTING
ANALYTES LIMITS
Ammonia Nitrogen (non distilled) 0.10
Chloride 1.0
Nitrate+Nitrite Nitrogen 0.020
Phosphorus, total 0.020
Sulfate 1.0
TKN 2.0
TOC (NPOC) 1.0
Total Alkalinity as CaCO3 1.0
VOA, Fatty Acids (9) 1.5
USEPA
METHOD
350.3
9251/325.2
353.2
365.2
9038/375.4
351.2
415.1/9060
310.1
5560C ..
SEE ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
Eckenfelder Laboratory, LLC
V WO---=--:::-.,
D. Rick Davis
Vice President
98003128
EB5598
05/05/98
UNITS CONC
mg/L u
mg/L u
mg/L u
mg/L u
mg/L u
mg/L u
mg/L u
mg/L u
mg/L u
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g
0
0
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ANALYTICAL REPORT NOTES, TERMS AND QUALIFIERS (INORGANIC)
Notes:
The metals and cyanide reporting limits (RLs) have been statistically determined to be no
less than three standard deviations as defined in 40 CFR 136, Appendix B, Revision 1.11. All
other reporting limits are referenced from the specific analytical method.
Terms:
NA Not Applicable
NR Not Requested
U Below Reporting Limits
Qualifiers:
B The reported value is less than the practical quantitation limit (PQL, project
defined) but greater than or equal to the RL.
E
N
w
*
**
(1)
(2)
The reported value is estimated due to the presence of matrix interference.
Predigested spike recovery not within control limits.
Post digestion spike recovery not within control limits.
RPD or absolute difference for Dup,licate analysis not within control limits.
Reference Standard Methods 17th edition.
pH analyzed outside USEPA specified holding time. pH must be measured
immediately after sample collection.
The sample pH did not meet the preservation guidelines. Therefore the pH was
adjusted upon receipt.
(3) The sample had to be diluted because of matrix interferences.
(4)
(5)
(6)
(7)
(8)
(9)
Reference Standard Methods 17th edition for the distillation method.
The sample was analyzed out of the USE PA holding time.
The sample was received in the laboratory out of the USE PA holding time.
The shipping cooler temperature exceeded 6°C upon receipt to Eckenfelder
Laboratory, LLC.
When the concentration of the analyte is below the detection limit, the detection
limit must be divided by the %Solids (in decimal form) in order to obtain the
sample's true detection limit on a dry weight basis.
Analysis was subcontracted
L:\REPORTS\ART&QIN2.DOC
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k ----r ECKENFELDER INC'
CLIENT: El Paso Energy Co.
DATE SAMPLED: 12/18/98
DATE RECEIVED: 12/23/98
DATE REPORTED: 01/08/98
CLIENT SAMPLE DESCRIPTION
ANALYTES DETECTION
• LIMITS
Methane 0.015
Ethane 0.005
Ethylene 0.005
#60313.006
W-28I W-AD
CONC CONC
1.5 1.5
0.24 0.14
0.43 0.025
ALL RESULTS EXPRESSED IN MICROGRAMS/LITER
UNLESS OTHERWISE NOTED.
•=ANALYSIS WAS SUBCONTRACTED.
ECKENFELDERIN
7)
D. RICK DAVIS
VICE PRESIDENT/ANALYTICAL & TESTING SERVICES
227 French Landing Drive
Nashville, Tennessee 37228
615.255.2288
FAX [phone]
W-17S
CONC
1.9
0.12
0.060
W-32I
CONC
0.52
0.097
0.061
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CLIENT: El Paso Energy Co.
DATE SAMPLED: 12/19/98 & 12/20/98
DATE RECEIVED: 12/23/98
DATE REPORTED· 01/08/98
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION
ANALYTES DETECTION
• LIMITS
Methane 0.015
Ethane 0.005
Ethylene 0.005
ECKENFELDER INC'?
#60313.006
9812182-01 9812182-02
W-30I W-10I
CONG CONG
1.4 1.6
0.095 0.016
0.46 0.010
ALL RESULTS EXPRESSED IN MICROGRAMS/LITER
UNLESS OTHERWISE NOTED.
'= ANALYSIS WAS SUBCONTRACTED.
227 French Landing Drive
Nashville, Tennessee 37228
615.255.2288
FAX [phone]
9812182-03 9812182-04 9812182-05
W-5I W-29I W-AC
CONG CONG CONG
0.56 0.26 0.24
0.15 0.019 0.017
0.36 0.009 0.009
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ECKENFELDER INC.®
CLIENT: El Paso Energy Co. #60313.006
DATE SAMPLED: 12/15/98 & 12/16/98
DATE RECEIVED: 12/23/98
DATE REPORTED: 01/08/98
CLIENT SAMPLE DESCRIPTION W-22S
ANALYTES DETECTION
• LIMITS CONG
Methane 0.015 0.26
Ethane 0.005 0.013
Ethylene 0.005 0.011
ALL RESULTS EXPRESSED IN MICROGRAMS/LITER
UNLESS OTHERWISE NOTED.
•=ANALYSIS WAS SUBCONTRACTED.
W-221
CONG
1.1
0.013
0.011
II l)'~\&"lJ =
D. RICK DAVIS
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VICE PRESIDENT/ANALYTICAL & TESTING SERVICES
W-AE
CONG
1.3
0.073
0.033
W-1S
CONG
0.14
0.011
0.007
W-20S
CONG
0.097
0.014
<0.005
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #60313.006
DATE RECEIVED: 01/28/99
DATE REPORTF.D· 02/04/99 -.
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION/SAMPLING DATE
REPORTING USEPA
ANALYTES LIMITS METHOD
Iron 50 6010B
Manganese 5.0 6010B
Alkalinity, Total (As CaCO3) 1.0 310.1
Chloride 1.0 9251
Nitrate+ Nitrite (as N) 0.020 353.2
Sulfate 1.0 9038
TOC (NPOC), Soluble 1.0 415.2
Methane (9) 0.015 NA
EthanP. (9) 0.0050 NA
Ethene (9) 0.0050 NA
Volatile Fatty Acids (9) 3.0 NA
See attached page :or de'inltlon of tenns and qualifiers.
227 French Landing Drive
Nashville, Tennessee 37228
6 I 5.255.2288
FAX [phone]
9901121-os I
W-BA
1/27/99
12:05:00 PM
UNITS CONC
µg/L . u
µg/L u
mg/L u
mg/L u
mg/L 0.21
mg/L u
mg/L u
µg/L 1.0
µg/L 0.043
µg/L 0.079
mg/L u
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #60313.006
DATE RECEIVED: 01/28/99
DATE REPORTED· 02/04/99
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION/SAMPLING DATE
REPORTING USEPA
ANALYTES LIMITS METHOD
Iron 50 6010B
Manganese 5.0 6010B
Alkalinity, Total (As CaCO3) 1.0 310.1
Chloride 1.0 9251
Nitrate+ Nitrite (as N) 0.020 353.2
Sulfate 1.0 9038
TOC (NPOC), Soluble 1.0 415.2
Methane (9) 0.015 NA
Ethane (9) 0.0050 NA
Ethene (9) 0.0050 NA
Volatile Fatty Acids (9) 3.0 NA
See attached page for definitions of tenns and qualifiers.
9901121-07
W-24S
1/27/99
2:15:00 PM
UNITS CONC
µg/L 56000
µg/L 1800
mg/L 14
mg/L 29
mg/L 0.60
mg/L 3.3
mg/L 1.2
µg/L 51
µg/L u
µg/L 0.041
mg/L 3.0
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #60313.006
DATE RECEIVED: 01/28/99
DATE REPORTED: 02/04/99
ECKENFELDER SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION/SAMPLl:>IG DATE
REPORTING USEPA
ANALYTES LIMITS METHOD
Iron 50 6010B
Manganese 5.0 6010B
Alkalinity, Total (As CaCOJ) 1.0 310.1
Chloride 1.0 9251
Nitrate+ Nitrite (as N) 0.020 353.2
Sulfate 1.0 9038
TOC (NPOC), Soluble 1.0 415.2
Methane (9) 0.015 NA
Ethane (9) 0.0050 NA
Ethent1 (9) 0.0050 NA
Volatile Fatty Acids (9) 3.0 NA
See attached page for definitions of tenns and qualifiers.
Eckenfelder Laboratory, LLC
D. Rick Davis
Vice President/Analytical & Testing Services
9901121-08
W-BB
1/27/99
2:15:00 PM
UNITS CONC
µg/L 57000
µg/L 1800
mg/L 18
mg/L 31
mg/L 0.58
mg/L u
mg/L u
µg/L 0.15
µg/L u
µg/L 0.033
mg/L 3.0
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Eckenfelder Laboratory, LLC
CLIENT: El Paso Energy #60316.006
DATE SAMPLED: 11/19/98
DATE RECEIVED: 11/20/98
DATE REPORTED· 12/9/98
ECKENFELDER SAMPLE NUMBER! 9811157-01
CLIENT SAMPLE DESCRIPTION W-31s
ANALYTES DETECTION
LIMITS CONC
Methane 3.0 11.6
Ethylene 0.005 7.6
Ethane 0.005 1.2
ALL RESULTS EXPRESSED IN MICROGRAMS/LITER
UNLESS OTHERWISE NOTED.
• = ANALYSIS WAS SUBCONTRACTED.
ECKENFELDER INC.
D. RICK DAVIS
9811157-02
W-31s
Duplicate
CONC
11.5
5.9
1.2
9811157-03
EB@
W-31i
CONC
1.0
2.4
0.099
VICE PRESIDENT/ANALYTICAL & TESTING SERVICES
227 French Landing Drive
Nashville, Tennessee 37228
615.255.2288
FAX [phone]
9811157-04 9811174-01
W-31i W-32i
CONC CONC
0.18 0.20
1.8 1.4
0.022 0.023
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ECKENFELDER INC.®
clENT: El Paso Energy #60313.006
D E RECEIVED: 11/20/98
D E REPORTED: 12/11/98
E EN FELDER SAMPLE NUMBE.R Cf NT SAMPLE DESCRIPTION/SAMPLING DATE
REPORTING USEPA
ANALYTES LIMITS METHOD
Alkalinity, Total (As CaCO3) 1.0 310.1
tmonia, Non-Distilled (as N) (9) 0.10· 350.3
Chloride 1.0 9251
Nitrate+ Nitrite (as N) 0.10 353.2 I Phosphorus, Total (as P) (9) 0.10 365.2
Sulfate 1.0 9038
TOC (NPOC), soluble 2.0 415.2
Volatile Fatty Acids (9) 3.0 NA
S ATTACHED PAGE FOR DEFINITION OF TERMS AND QUALIFIERS
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9811157-01
W-31S
11/19/98
11:45:00 AM
UNITS CONC
mg/L 61
mg/L u
mg/L 4.6
mg/L u
mg/L 0.16
mg/L 9.1
mg/L u
mg/L u
9811157-02 9811157-03 9811157-04
W-31S Dupe EB@ W-31i WB-31 I
11/19/98 11/19/98 11/19/98
11:45:00 AM 12:45:00 PM 3:55:00 PM
CONC CONC CONC
55 u 34
u u u
4.6 u 1.1
u u 0.50
0.29 u u
10 u 11
u u u
u u u
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ECKENFELDER INC.®
CLIENT: El Paso Energy #60313.006
DATE RECEIVED: 11/21/98
DATE REPORTED: 12/11/98
ECKENFELDE~ SAMPLE NUMBER
CLIENT SAMPLE DESCRIPTION/SAMPLING DATE
REPORTING
ANALYTES LIMITS
Alkalinity, Total {As CaCO3) 1.0
Ammonia, Non-Distilled (as N) (9) 0.10
Chloride 1.0
Nitrate+ Nitrite (as N) 0.10
Phosphorus, Total (as P) (9) 0.10
Sulfate 1.0
TKN 0.20
TOC (NPOC), soluble 2.0
Volatile Fatty Acids (9) 3.0
USEPA
METHOD
310.1
350.3
9251
353.2
365.2
9038
351.2
415.2
NA
SEE ATTACHED PAGE FOR DEFINITION DF TERMS AND QUALIFIERS
ECKENFELDER INC.
D. RICK DAVIS
VICE PRESIDENT/ANALYTICAL & TESTING SERVICES
9811174-01
W-32i
11 /20/98
8:30:00 AM
UNITS CONC
mg/L 65
mg/L u
mg/L 1.7
mg/L 0.59
mg/L u
mg/L 14
mg/L u
mg/L u
mg/L 3.0
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ECKENFELDER IN~
CLIENT: El Paso Energy Co. #60313.006
DATE SAMPLED: 12/17/98
DATE RECEIVED: 12/23/98
DATE REPORTED: 01/08/98
ECKENFELDER SAMPLE NUMBER 9812163-01 9812163-02
CLIENT SAMPLE DESCRIPTION AA121798 W-24S
ANALYTES DETECTION
• LIMITS CONC CONC
Methane 0.015 6.5 2.1
Ethane 0.005 0.14 0.14
Ethylene 0.005 0.028 0.044
ALL RESULTS EXPRESSED IN MICROGRAMS/LITER ·
UNLESS OTHERWISE NOTED.
•=ANALYSIS WAS SUBCONTRACTED.
227 French Landing Drive
Nashville, Tennessee 3722&
6 I 5.255.2288
FAX [phone]
9812163-03 9812163-04 9812163-05
W-5S W-8I W-26I
CONC CONC CONC
6.2 0.77 1.3
0.30 0.15 0.16
0.024 27 1.3
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ECKENFELDER INC.®
CLIENT: El Paso Energy Co. #60313.006
DATE S/.MPLED: 12/15/98 & 12/16/98
DATE RECEIVED: 12/23/98
DATE REPORTED: 01/08/98
CLIENT SAMPLE DESCRIPTION W-18S
ANALYTES DETECTION
• LIMITS CONC
Methane 0.015 0.37
Ethane 0.005 0.10
Ethylene 0.005 0.006
ALL RESULTS EXPRESSED IN MICROGRAMS/LITER
UNLESS OTHERWISE NOTED.
'= ANALYSIS WAS SUBCONTRACTED.
I ECKENFELDER INC.
L) 0l CJ~ I D. RICK DAVIS
W-19S
CONC
0.34
0.083
0.012
VICE PRESIDENT/ANALYTICAL & TESTING SERVICES
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W-9S
CONC
0.51
0.12
0.009
W-20D
CONC
4.1
0.26
0.43
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ECKENFELDER INC!
CLIENT: El Paso Energy Co. #60313.006
DATE SAMPLED: 12/15/98 & 12/16/98
DATE RECEIVED: 12/23/98
DATE REPORTED: 01/08/98
ECKENFELDER SAMPLE NUMBER 9812156-01 9812156-02
CLIENT SAMPLE DESCRIPTION
ANALYTES DETECTION
* LIMITS
Methane 0.015
Ethane 0.005
Ethylene 0.005
ALL RESULTS EXPRESSED IN MICROGRAMS/LITER
UNLESS OTHERWISE NOTED.
•=ANALYSIS WAS SUBCONTRACTED.
W-20I W-31I
CONC CONC
1.4 0.80
0.22 0.21
0.55 0.019
227 French Landing Drive
Nashville, Tennessee 37228
615.255.2288
FAX [phone]
9812156-03 9812156-04
W-12I W-31S
CONC CONC
2.2 3.8
0.26 0.27
0.028 0.015
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ECKE~FELDER INC.®
CLIENT: El Paso Energy Co. #60313.006
I DATE SAMPLED: 12/15/98 & 12/16/98
DATE RECEIVED: 12/23/98
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DATE REPORTED: 01/08/98
CLIENT SAMPLE DESCRIPTION
ANALYTES DETECTION
• LIMITS
Methane 0.015
Ethane 0.005
Ethylene 0.005
ALL RESULTS EXPRESSED IN MICROGRAMS/LITER I UNLESS OTHERWISE NOTED.
•~ANALYSIS WAS SUBCONTRACTED.
I
D. RICK DAVIS
W-AA
CONC
3.3
0.23
0.011
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VICE PRESIDENT/ANALYTICAL & TESTING SERVICES
W-AB
CONC
2.1
0.23
0.032
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I ANALYTICAL REPORT TERMS AND QUALIFIERS {ORGANIC)
I CRQL: Contract required quantitation limit.
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U:
B:
D:
E:
J:
The presence of a "U" indicates that the analyte was analyzed for but
was not detected or the concentration of the analyte quantitated below
the CRQL.
The presence of a "B" to the right of an analytical value indicates that
this compound was also detected in the method blank and the data
should be interpreted with caution. One should consider the possibility
that the correct sample result might be less than the reported result and,
perhaps, zero.
When a sample (or sample extract) is rerun diluted because one of the
compound concentrations exceeded the highest concentration range for
the standard curve, all of the values obtained in the dilution run will be
flagged with a "D".
The concentration for any compound found which exceeds the highest
concentration level on the standard curve for that compound will be
flagged with an "E". Usually the sample will be rerun at a dilution to
quantitate the flagged compound.
The presence of a "J" to the right of an analytical result indicates that the
reported result is estimated. The mass spectral data pass the
identification criteria showing that the compound is present, but the
calculated result is less than the CRQL. One should feel confident that
the result is greater than zero and less than the EQL.
L:\REPORTS\CRQLCLP.DOC
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APPENDIX F-3
DA TA VALIDA TI ON REPORT DA TED
AUGUST 24, 1998
\ \,TN\SYS\DATA \PROJ\03 IJ.08\PDI-CVR.DOC
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DAT A VALIDATION REPORT
FCX Statesville
Prepared By
Environmental Data Services, Ltd.
For
Eckenfelder, Inc.
August 24, 1998
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I DAT A ASSESSMENT NARRATIVES
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DATA ASSESSMENT NARRATIVE FOR VOLATILES
SITE: FCX Statesville
LABORATORY: Eckenfelder, Inc.
SAMPLE DELIVERY GROUP: FCX-V2991
This sample delivery group consists of the following water samples:
W-12S W-12I W-18S ' W-30I
W-20I W-20S FB42998 TB 1021 & 1022
W-20S DUPE EB42998 W-22I W-29I
W-9S DUPE PurQe Water W-28I W-19S
FB5598 EB5598 TB 1022 & 1 023 Hid□. Blk. 050798
W-10I
W-5S
Hldn. Blk. 050698
W-5I
W-22S
W-24S
W-9S
W-17S
Samples described above were analyzed via USEPA Low Level CLP SOW OLCD1 .D to determine the
concentration of volatiles in water.
USEPA Contract Laboratory Program National Functional Guidelines for Organic Data Review (February
1994) have been considered during the validation of this data and in determining its usability.
All data are valid and acceptable except those analytes which have been qualified as described in the
attached glossary. All data qualification related to this group of samples is detailed on the attached
sheets.
Major Data Quality Issues
None.
Minor Data Quality Issues
Blank Contamination• Various common laboratory contaminants were present in method, field and trip
blanks associated with samples in this delivery group. Effected compound results have been
qualified per USEPA guidelines.
Mass Spectrometer Tuning• Several sample analysis reported were based on analyses associated with
non-compliant instrument tunes. The validator has elected to flag all data reported from the
effected analyses as estimated.
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Two facts should be noted by all data users. First, the "R" flag means that the associated value is
unusable due to significant QC problems, the data is invalid and provides no infonnation as to whether
the compound is present or not. "R" values should not appear on any data tables even as a last resort.
Lastly, strict QC serves to increase confidence in data but any value potentially contains error.
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HOLDING TIME
The amount of an analyte can change with time due to chemical instability, degradation, volatilization, etc.
If the specified holding time is exceeded the data may not be valid.
The analyses perfom,ed on samples in this sample delivery group were all done within established
holding times.
BLANK CONTAMINATION
Quality assurance blanks, method, trip, field, or rinse blanks are prepared to identify any contamination
which may have been introduced into the samples during preparation or field activity. Method blanks
measure lab contamination. Trip blanks measure cross contamination during shipment. Field and rinse
blanks measure cross contamination during field operations.
Method Blank Contamination
Method blanks were analyzed at the proper frequency. Upon examination, the method blanks did not
contain any target analyte at or above reportable concentration levels with the following exception:
The method blank analyzed on 5/11/98 (V1 BLK0511) was found to contain acetone at a concentration of
1.6 ppb. Sample Purge Water 5-6-98 was associated with the method blank described above.
Larger amounts of acetone were found in the field blank associated with the purge water sample.
Therefore the acetone value was qualified based on the amount of acetone found in the field blank.
Field Blank/Trip Blank Contamination
Field, trip and equipment blank sets were collected on 4-29-98 and 5-5-98.
Acetone was found in the blanks collected on 4-29-98. The equipment blank contained acetone at 3.1
ppb. The field blank contained acetone at 1. 7 ppb. The trip blank contained acetone at 2.3 ppb. Per
validation guidelines samples associated with the blanks described above were qualified based on the
highest concentration blank. The following samples were associated with the blank samples collected on
4-29-98 and were found to contain comparable levels of acetone i.e. (less than 1 Ox the concentration of
the blank). Acetone results for the samples listed have been flagged ·u· not detected.
W-12S W-18S W-30I W-10I W-22S W-20I
W-20S W-5S W-24S W-20 DUP W-29I
Acetone, mett,ylene chloride and/or toluene were positively identified in the blanks collected on 5-6-98.
Concentrations of contaminants observed in the blanks are listed below:
Blank Acetone Methylene Toluene
Chloride
Trip Blank /5-6-98\ 2.5 oob 0.31 oob ND
Field Blank (5-5-98) 3.5 oob 0.38 nnb 0.21 nnb
Equipment Blank (5-5-98) 2.8 ppb 0.37 DDb 0.19DDb
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The following samples were associated with the blank samples listed above:
II W-9S I W-9 DUP I Purge Water I W-28I I W-19S I W-5I I W-17S
Only the purge water sample contained levels of toluene comparable to that found in field blank 5-5-98
and therefore has been flagged "U" not detected. Likewise, sample W-17S has been qualified not
detected for methylene chloride and samples W-9 DUP, Purge Water and W-5I were flagged "U" for
acetone.
MASS SPECTROMETER TUNING
Tuning and performance criteria are established to ensure adequate mass resolution, proper identification
of compounds, and to some degree, sufficient instrument sensitivity. These criteria are not sample
specific. Instrument performance is determined using standard materials. Therefore, these criteria should
be met in all circumstances.
The tuning standard for volatiles is bromofluorobenzene (BFB).
The majority of tunes associated with this SDG were fully compliant. The following are exceptions:
Three instrument tuning standard evaluations failed to meet method acceptance criteria.
I Tune I Criteria I
5/7/98 17:22 mass 174/175 ion ratio
5/8/98 09:09 mass 176/177 ion ratio
5/11/98 09:36 mass 176/177 ion ratio
The following samples had results reported based on analyses associated with one of the non-compliant
instrument tunes listed above.
I Sample I Results Effected
W-20I All
W-5S All
Purge Water All
Holdinq Blank (5-7-98) All
W-12I Acetone
Results effected for the samples listed have been qualified as "J" estimated.
CALIBRATION
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Satisfactory instrument cali'Jration is established to ensure that the instrument is capable of producing
acceptable quantitative results. The initial calibration curve demonstrates that the instrument is capable of
giving acceptable performance at the beginning of an analytical sequence. The continuing calibration
verifies that the instrument is giving satisfactory daily performance.
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Response Factor
The response factor measures the instruments responses to specific chemical compounds. The response
factors for the VOA Target Compound List must be greater than or equal to 0.05 in both the initial and
continuing calibrations. A value less than 0.05 indicates serious detection and quantitation problems.
RRF values in all initial and continuing calibrations were greater than 0.05.
Percent Relative Standard Deviation (RSD) and Percent Deviation (%DJ
Percent RSO is calculated from the initial calibration and is used to indicate stability of a specific
compound·over the calibration range. %0 compares the response factor of the continuing calibration with
the mean response factor of the initial calibration. Therefore %0 is a measure of the instruments daily
performance.
The following QC criteria has been applied for this project:
% RSD of initial calibration must be <30.0 %
% D for continuing calibrations must be <25.0%
A value outside these limits indicates potential detection and quantitation errors. According to Region tit
modifications (Sept., 1994) alt positive results are fiagged as estimated, and non detects are not fiagged
except in situations where there is a gross difference i.e. 50% or greater and then professional judgment
takes precedence.
The initial and continuing calibrations associated with this sample delivery group met all validation criteria
with one exception. The initial calibration performed on 5/11/98 (VOA 1) had an observed % RSO value
for bromofonm (30.4%) that exceeded validation toluene limits. No associated sample analyses yielded a
positive value for bromoform. Therefore no qualification of data was necessary.
INTERNAL STANDARDS PERFORMANCE
Internal standard perfonmance criteria is meant to ensure that the GC/MS sensitivity and response are
stable during every experimental run.
The internal standard area count must not vary by more than a factor of two from the associated
continuing calibration standard. The retention time of the internal standard must not vary by more than+/-
30 seconds from the associated continuing calibration standard. If the area count is outside the (-50% -
100%) range of the associated standard, all positive results for compounds quantitated using that
standard are qualified as estimated, and non detects as UJ, but only if area is< 50%.
Internal standard recoveries observed in all samples and method blanks were within acceptable limits.
SURROGATES
All samples and blanks are spiked with surrogate compounds prior to sample preparation and analyses to
evaluate overall laboratory performance and efficiency of the analytical technique.
All samples and method blanks evaluated in this report had observed surrogate recoveries within the
established limtts.
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COMPOUND IDENTIFICATION
Volatile
TCL compounds are identified on the GC/MS by using the analyte's relative retention time (RRT) and ion
spectra. For the results to be a positive hit, the sample peak must be within:: 0.06 RRT units of the
standard compound, and have an ion spectra which has a ratio of the primary and secondary ion
intensities within 20% of that in the standard compound. No analytes were qualified for compound
identification.
MATRIX SPIKE/MATRIX SPIKE DUPLICATE
The matrix spike and matrix spike duplicate are generated to detenmine the precision and accuracy of the
analytical procedure in a given matrix. This infonmation may be used to qualify data.
Sample W-20S was analyzed as matrix spike/matrix spike duplicate pair. Upon evaluation all precision
and accuracy indicators were favorable. No significant matrix interferences were apparent.
Laboratory control samples were processed at a frequency of one per twelve hour analysis period. LCS
recoveries were well within acceptance· limits in every case.
OTHER QC DATA OUT OF SPECIFICATION
None.
FIELD DUPLICATE
Samples (W-9S and W-9S Dup) and (W-20S and W-20S Dup) comprise the field duplicate pairs
associated with samples in this delivery group. Field precision exhibited was extremely good. The
largest percent difference observed for positively identified target analytes between either pair was 11%.
Field precision was demonstrated to be well within acceptable tolerances.
SYSTEM PERFORMANCE AND OVERALL ASSESSMENT
Non-compliant instrument tuning and control blank contamination data quality issues were found to
impact the results reported. All other QC criteria appears to be acceptable.
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DATA ASSESSMENT NARRATIVE FOR METALS
SITE: FCX Statesville
LABORATORY: Eckenfelder, Inc.
Validation Report: FCX 0313.05
This sample delivery group consists of the following water samples:
W-11S W-6S DUPE W-6S W-12S
W-30! W-22S W-10I W-20I
W-5S W-24S W-20S DUPE EB42998
W-9S W-9S DUPE PURGE WATER W-28I
W-16S W-16I W-17S FB5598
W-12I
W-20S
W-22I
W-19I
EB5598
W-18S
FB42998
W-29I
W-5I
The samples described above were analyzed for either total target analyte list metals or manganese and
iron as directed on the field coc. The analyses were performed based on methodologies outlined in the
USEPA CLP SOW 3/90.
"USEPA Contract Laboratory Program National Functional Guidelines for inorganic Data Review" (Feb.,
1994) were used to evaluate the data set.
All data are valid and acceptable except those analytes which have been qualified with a "J" (estimated),
or "R" (unusable). All action is detailed on the attached sheets.
Major Data Quality Issues
Calibration -The calibration associated with all mercury results reported was performed several weeks
prior to sample analysis. Per the specified validation guidance document all mercury results
have been flagged "R" unusable.
Minor Data Quality Issues
Matrix Spike Recovery -Recovery of matrix spike additions of metal analytes to a representative sample
were not acceptable for several analytes. Associated sample results for the effected elements
have been qualified as estimated.
ICP Serial Dilution -One analyte had an observed percent deviation value that fell outside val_idation
acceptance limits during the ICP serial dilution determination. Sample results associated with
the non-compliant serial dilution determination have been qualified as estimated.
Duplicate -One analyte exhibited unacceptable precision during one MS/MSD determination. Per
validation guidelines results for the effected analyte in associated sample have been flagged "J"
estim· ted.
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Two facts should be noted by all data users. First, the "R" flag means that the associated value is
unusable. In other words, due to significant QC problems, the analysis is invalid and provides no
information as to whether the compound is present or not. "R" values should not appear on data tables
even as a last resort. The second fact to keep in mind is that no analyte concentration, even if it has
passed all QC tests, is guaranteed to be accurate. Strict QC serves to increase confidence in data but
any value potentially contains error.
list/Director
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HOLDING TIME
The amount of an analyte in a sample can change with time due to chemical instability, degradation,
volatilization, etc. If the specified holding time is exceeded the data may not be valid. Those analytes in
the samples whose holding time has been exceeded will be qualified as estimated, or unusable when
grossly exceeded.
All analyses were completed well within acceptable holding times.
BLANK CONTAMINATION
Quality assurance blanks, method, trip, field, or rinse blanks are prepared to identify any contamination
which may have been introduced into the samples during sample preparation or field activity. Trip blanks
measure cross contamination during shipment. Field and rinse blanks measure cross contamination
during field operations.
Method Blank Contamination
Method blanks were evaluated at the proper frequency. The associated method blanks provided data
indicating no contamination was present.
Field or Rinse Blank Contamination
Rinse blank and equipment blank samples were collected on every other day during field sample
collection. Upon evaluation of the field and equipment blank data obtained, no analytes were found to
be present at levels above the CRDL in any associated field or equipment blank.
CALIBRATION
Satisfactory instrument calibration is established to ensure that the instrument is capable of producing
acceptable quantitative data. The initial calibration curve and its verific,. tion demonstrates that the
instrument is capable of giving acceptable performance at the beginning of the analytical sequence. The
continuing calibration verification standards provide information as to the continuing stability of the
calibration curve.
Instrument calibrations must be successfully performed daily or once every 24 hours and each time the
instrument is set up. The ICP was calibrated at the proper frequency during the analyses of samples
from the delivery group. The cold vapor instrument (Hg) however was calibrated on 4/22/98 and
samples were analyzed on 5/6/98 and 5/15/98. Per validation guidelines all mercury results for samples
in this delivery group have been flagged "R" unusable.
Correlation Coefficient
All calibrations associated with the data represented here demonstrated satisfactorily that all criteria were
met.
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Initial and Continuing Calibration Verification
All initial and continuing calibration verifications that bracketed sample analyses associated with the
sample delivery group were within acceptance limits.
Initial and Continuing Calibration Blanks
All initial and continuing calibration blanks (ICP only) were evaluated and none associated with reported
sample results had observed analyte concentrations greater than the reported detection limits (positive or
negative). No continuing calibration blanks were analyzed during the mercury analytical sequences.
Since all mercury results were previously rejected due to improper calibration, no further qualification of
data was necessary.
MATRIX SPIKE
The matrix spike is generated to detenmine the long tenm accuracy of the analytical method in a given
matrix. The matrix spike percent recoveries may be used to qualify data. The following analytes in the
samples shown were qualified due to matrix spike determinations:
Sample W-5S was analyzed as a matrix spike and matrix spike duplicafe pair for total tarret analyte
metals except mercury. The result of this evaluation was that all elements had observed spike recovery
within the limits with the following exceptions:
Aluminum
Selenium
Thallium
TOTAL
-55.7%
67.4%
146.5%
-57.4%
64.2%
126.5%
The following samples are associated with the matrix spike recoveries listed above:
Ii W-SS J W-11 S J W-6S J W-6S DUP
Total metals sample results for the elements listed above except thallium have been qualified as
estimated. Thallium was not qualified as estimated ,since high bias was observed and all thallium sample
results were not detected.
Sample W-17S was analyzed as a matrix spike and matrix spike duplicate pair for total metals (TAL list
except Hg). The result of this evaluation was that all elements had observed spike recovery within the
specified acceptance limits.
Sample W-6S was analyzed as a matrix spike and matrix spike duplicate pair for mercury. Observed
percent recovery values were well within acceptable limits in both cases.
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DUPLICATE
Precision between MS/MSD pairs was evaluated for samples W-SS and W-17S for all analytes except
mercury. All precision indicators were favorable during the evaluation of sample W-17S. Likewise all
relative percent difference values for W-SS fell within allowable limits with the exception of lead. Lead
results for the following samples were associated with the ·w-ss duplicate determination and have been
flagged "J' estimated.
Ii W-5S I W-11 S I W-6S I W-6S DUP
Sample W-6S was analyzed as a matrix spike and matrix spike duplicate pair for mercury. The result of
this evaluation was that the mercury duplicate pair had an observed percent difference within the
allowable limits.
LABORATORY CONTROL SAMPLE
The Laboratory Control Sample is a quality control sample of known concentration which is processed
along with a batch of samples. The percent recovery of the LCS can be used to assess the accuracy of
the analytical procedure performed by a specific individual. during a specific time period, and utilizing the
same reagents and equipme'nt as those used for sample analyses. The LCS data is independent of
sample matrix and the results may formulate a basis for qualification.
All associated laboratory control samples had observed percent recoveries well within the range
required.
ICP SERIAL DILUTION
Precision between diluted, and non-diluted analyses was determined on sample W-SS. All metal
analytes met validation acceptance limits.
Precision between diluted and non-diluted analyses was determined on sample W-17S. All metal
analytes met validation acceptance limits with the exception of aluminum. The results for the effected
element in the following samples have been qualified as estimated:
FB 5598 W-9S W-9S DUP PURGE WATER
W-16S W-16I W-17S EB 5598
CRDL
CRDL (2 times the CRDL) standards were analyzed as required during ICP analytical run sequences.
Upon evaluation one each selenium, lead and thallium standard recoveries were slightly higher than the
highest acceptable validation limit. The validator elected not to apply any optional qualifiers to the data
set based on the minor CRDL excursion.
The laboratory failed to analyze the required CRA standard (1 times CRDL) during the mercury analytical
sequences. All mercury data was previously qualified "R' no further qualification of mercury data was
necessary.
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INTERFERENCE CHECK STANDARDS
One ICP analytical run sequence did not contain a required final ICSA/ICSAB determination. A facility
power failure caused the deficiency. Since none of the ICSA analytes were present in the associated
samples in the effected concentration range, no qualification of data was necessary based on the
anomaly.
FIELD DUPLICATE
Samples 0N-9S/W-9S DUPE) and ry,J-6S/W-6S DUPE) comprise the field duplicate pairs associated
with this sample delivery group. The following table lists the relative percent difference values for each
(positive at the CRDL results only) of the field duplicate pairs.
W-9S
Analvte RPD
Aluminum 78
Chromium 12
Iron 77
Manqanese 37
zinc 9.2
W-6S
Analvte RPO
Aluminum 4.3
Chromium 40
Cobalt 5.4
Iron 5.3
Lead 11
Manqanese 6.2
Sodium 1.3
zinc 9.7
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SYSTEM PERFORMANCE AND OVERALL ASSESSMENT
The laboratory attempted to perform the analyses evaluated according to USEPA CLP SOW 3/90. The
following are procedural deficiencies not directly impacting data quality and therefore not previously
discussed. ·
1. No more than 20 field samples should be included in a single sample delivery group. This SDG
contains 25 environmental samples and four field blanks.
2. Instrument detection limits should be derived according to the method specified procedure prior
to sample analysis. Samples analyzed May, 1998 IDL performed July, 1998.
3. Several final results were reported incorrectly. The following should be considered when
reporting form I results: Enter "B" if the reported value was obtained from a reading that was
less than the CRDL but greater than the IDL. If the analy1e was analyzed for but not detected
above the IDL, a "U" should be entered. Several negative sample results were corrected by the
validator individual "U" at the IDL value.
Please note, samples analyzed for target analy1e metals were acid digested using 50 ml of sample and a
final volume of 25 ml thereby increasing method sensitivity by a factor of 2. However, it should be
understood that per the analy1ical method a 100 ml aliquot should be digested with a final volume of 100
ml.
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J -
R -
N -
JN -
UJ -
GLOSSARY OF DATA QUALIFIERS
The material was analyzed for, but not detected. The associated numerical value is the sample
quantitation limit.
The associated numerical value is an estimated quantity.
The data are unusable (compound may or may not be present).
Presumptive evidence of the presence of the material.
Presumptive evidence of the presence of the material at an estimated concentration.
The material was analyzed for, but was not detected. The sample quantitation limit is an
estimated quantity.
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LABORATORY DAT A WITH QUALIFIERS ADDED
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FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-12S
Lab Name: ECKENFELDER INC. .Contract: EL PASO ENERGY
rJ Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V2991
~trix: (soil/water)
1'mple wt/vol:
WATER
25.00 (g/mL) ML
LOW
Lab Sample ID: 98002991
Lab File ID: 2991RE
Date Sampled: 04/30/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
Soil Aliquot Volume:
Ijvel: (low/med)
.Moisture: not dee.
I Column: DB-624 ID: 0.53 (mm)
il Extract Volume: (uL) ----
1 CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
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67-64-1---------Acetone 5-o ;!,...-3-
71-43-2---------Benzene 1.0
75-27-4---------Bromochloromethane 1.0
75-27-4---------Bromodichloromethane 1.0
75-25-2---------Bromoform 1.0
74-83-9---------Bromomethane 1.0
78-93-3---------2-Butanone 5.0
75-15-0---------Carbon disulfide 1.0 -
56-23-5---------Carbon tetrachloride 1.0
108-90-7--------Chlorobenzene 1. 0
75-00-3---------Chloroethane 1.0
67-66-3---------Chloroform 1.0
74-87-3---------Chloromethane 1.0
124-48-1--------Dibromochloromethane 1.0
96-12-8---------1,2-Dibromo-3-chloropropane 1. 0
106-93-4--------1,2-Dibromoethane -1.0
95-50-1---------1,2-Dichlorobenzene 1.0
541-73-1--------1,3-Dichlorobenzene 1.0
106-46-7--------1,4-Dichlorobenzene 1.0
75-34-3---------1,1-Dichloroethane 1. 0
107-06-2--------1,2-Dichloroethane 1.0
75-~5-4---------1,1-Dichloroethene 1.0
156-59-2--------cis-l,2-Dichloroethene 1.0
156-60-5--------trans-l,2-Dichloroethene 1.0
78-87-5---------1,2-Dichloropropane --1.0
10061-01-5------cis-l,3-Dichloropropene 1.0
10061-02-6------trans-l,3-Dichloropropene 1.0
100-41-4--------Ethylbenzene --1.0
591-78-6--------2-Hexanone 5.0
75-09-2------• --Methylene chloride 0.61
108-10-1--------4-Methyl-2-pentanone 5.0
100-42-5--------Styrene 1. 0
79-34-5---------1,1,2,2-Tetrachloroethane __ 1.0
FORM I VOA
cf-
u u u
u u u u u u u
u
u u u u
u u u u u
u u u
u
u u u u
J
u u u
. I \..
00061
FORM 1 CLIENT SAMPLE NO. I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-12S
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
11atrix: (soil/wate.r)
lample wt/vol:
l·evel: (low/med)
• Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
a,c Column: DB-624 ID: 0.53 (mm)
'toil Extract Volume: (uL) ----
Lab Sample ID: 98002991
Lab File ID: 2991RE
Date Sampled: 04/30/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene 1. 0 u
108-88-3--------Toluene 1.0 u
71-55-6---------1,1,1-Trichloroethane 1.0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 1.0 u
75-01-4---------Vinyl chloride 1.0 u
1330-20-7-------Xylene(total) 1. 0 u
-
FORM I VOA
I
I
00066
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-12I
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
l trix: (soil/water)
mple wt/vol:
rve~: (low/med)
o Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
f= Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 98002992
Lab File ID: 2992
Date Sampled: 04/30/98
Date Analyzed: 05/07/98
Dilution Factor: 1.0
!oil Extract Volume: (uL) ----Soil Aliquot Volume: ____ (uL)
1
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1--~------Acetone 3/0 ~
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide -
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane
--
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene c:nloride
108 -10-1--

-

-
·· -

-
-4-Methyl-2-pentanone
100-42 -5--

-

-
·· -

-
-Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
Q
2-9-& -£-i) ~
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
5.0 u
0.39 J
1.0 u
1.0 u ! 1. 0 u '. 0.14 J
1.0 u
1.0 u
1. 0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1. 0 u
1. 0 u
1.0 u
1.0 u
1.0 u
5.0 u
2.0 u
1.1 J
1.0 u
1. 0 u
I
I
00067
FORM. 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-12I
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
lample wt/vol:
level: (low/med)
Moisture: not dee.
WATER
25. 00 (g/mL) ML
LOW
jC Column: DB-624 ID: o. 53 (mm)
Lab Sample ID: 98002992
Lab File ID: 2992
'oil Extract Volume: (uL) ----
Date Sampled: 04/30/98
Date Analyzed: 05/07/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
120-82-1--------1,2,4-Trichlorobenzene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total) -
FORM I VOA
Q 1/t1/;~J
1.5
0.24 J
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
I
I
00084
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-18S
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY 'b Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
._atrix: (soil/water)
&.mple wt/vol:
rve~: (low/med)
, Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
W: Column: DB-624 ID: 0. 53 (mm)
Lab Sample ID: 98002993
Lab File ID: 2993RE
Date Sampled: 04/30/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
!oil Extract Volume:· (uL) ----Soil Aliquot Volume: ____ (uL)
1
I
I
I
I
I
·I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide -
56-23-5---------carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-1,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1 1 2 2-Tetrachloroethane ' ' ' --
FORM I VOA
Q i/t 5i~S.,v1,
6.0 i./
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
3.4
5.0 u
1.0 u
1.0 u
I 00085
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I W-18S
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lb Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water) WATER
lmple wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW
I Moisture: not dee.
I Column: DB-624 ID: 0.53 (mm)
il Extract Volume: (uL) ----
Lab Sample ID: 98002993
Lab File ID: 2993RE
Date Sampled: 04/30/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
Soil Aliquot Volume: ----
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene 3.5
108-88-3--------Toluene 1. 0 u
71-55-6--

-

-

-

-

-

-
-1, 1, 1-T.richloroethane 1.0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 1.0 u
75-01-4---------Vinyl chloride 1. 0 u
1330-20-7-------Xylene(total) 1.0 u
FORM I VOA
(uL)
I 00091
FORM 1 CLIENT SAMPLE NO.
I
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-30I
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
tb Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (~ :,il/water) WATER
lmple wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW
IMoisture: not dee.
Lab Sample ID: 98002994
Lab File ID: 2994DRE1
Date Sampled: 04/30/98
Date Analyzed: 05/12/98
Dilution Factor: 2.5
I Column: DB-624 ID: 0. 53 (mm)
il Extract Volume: (uL) ----Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride -
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-1,2-Dichloroethene
156-60-5--------trans-1,2-Dichloroethene
78-87-5---------1,2-Dichloropropane
10061-(; 1-5--

-

-

-
-cis-1, 3 -Dichlorop'ropene
--
10061-02-6------trans-1,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------~ethylene chloride
108-10-1--------~-Methyl-2-pentanone
100-42-5--------Styrene
79-34-=---------l,1,2,2-Tetrachloroethane --
FORM I VOA
Q 7 /13( (/ fT;!-..
20 D i)
2.5 UD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
12 UD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
1.2 JD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
1.1 JD
20 D
0.38 JD
5.3 D
2.5 UD
2.5 UD
2.5 UD
12 UD
12 D
12 UD
2.5 UD
2.5 UD
I
I
00092
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-30I
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
lamp le wt/vol:
jevel: (low/med)
l Moisture: not dee.
WATER
25.00 (g/rnL) ML
LOW
a,c Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 98002994
Lab File 'ID: 2994DRE1
Date Sampled: 04/30/98
Date Analyzed: 05/12/98
~oil Extract Volume: (uL) ----
Dilution Factor: 2.5
Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------TetrachlorQethene Soo
108-88-3--------Toluene
71-55-6---------1 1 1-Trichloroethane ' ' . 79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
-
FORM I VOA
Q 1 [tJli~i'"
5-6-e flE-D
0.46 JD
2.5 UD
2.5 UD
34 D
2.5 UD
2.5 UD
I
I
00120
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-l0I
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.:. NA SDG No.: FCX.V2991
_-1atrix: (soil/water)
11,ample wt/vol:
WATER
25. 00 (g/mL) ML
LOW
Lab Sample ID: 98002995
Lab File ID: 2995RE
Date Sampled: 04/30/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
Soil Aliquot Volume:
revel: (low/med)
' -.-Moisture: not dee. re Column: DB-624 ID: 0. 53 (mm)
Soil Extract Volume: (uL) ----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L I
I
I
I
I
I
I
I
I
I
I
I
I
6"7-64-1---------Acetone -5;0~
71-43-2---------Benzene 1.0
75-27-4---------Bromochloromethane 1. 0
75-27-4---------Bromodichloromethane 1.0
75-25-2---------Bromoform 1. 0
74-83-9---------Bromomethane 1. 0
78-93-3---------2-Butanone 5.0
75-15-0---------Carbon disulb.de 1. 0
56-23-5---------Carbon tetrachloride
-1.0
108-90-7--------Chlorobenzene 1. 0
75-00-3---------Chloroethane 1.0
67-66-3---------Chloroform 1. 0
74-87-3---------Chloromethane 1.0
124-48-1--------Dibromochloromethane 1.0
96-12-8---------1,2-Dibromo-3-chloropropane 1. 0
106-93-4--------1,2-Dibromoethane -1.0
95-50-1---------1,2-Dichlorobenzene 1.0
541-73-1--------1,3-Dichlorobenzene 1.0
106-46-7--------1,4-Dichlorobenzene 1. 0
75-34-3---------1,1-Dichloroethane 1.0
107-06-2--------1,2-Dichloroethane 1. 0
75-35-4---------1,1-Dichloroethene 1.0
156-59-2--------cis-l,2-Dichloroethene 1.0
156-60-5--------trans-l,2-Dichloroethene 1.0
78-87-5---------1,2-Dichloropropane
--1.0
10061-01-5------cis-l,3-Dichloropropene 1.0
10061-02-6------trans-l,3-Dichloropropene 1.0
100-41-4--------Ethylbenzene --1.0
591-78-6--------2-Hexanone 5.0
75-09-2---------Methylene chloride 4.1
108-10-1--------4-Methyl-2-pentanone 5.0
100-42-5--------Styrene 1.0
79-34-5---------1,1,2,2-Tetrachloroethane __ 1.0
FORM I VOA
-0-u u u u u u u u u u u u u u u u u u u u u u u u u u u u
u u u
u
00121
FORM 1 CLIENT SAMPLE NO. I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-l0I
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
lample wt/vol:
ll'evel: (low/med)
I Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
.C Column: DB-624 ID: 0.53 (mm)
~oil Extract Volume: (uL) ----
Lab Sample ID: 98002995
Lab File ID: 2995RE
Date Sampled: 04/30/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I
I
I
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,1,l-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
0.66 J
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
I FORM 1
00127
CLIENT SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-22S
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water) WATER
lample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW
I Moisture: not dee.
jC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 98002996
Lab File ID: 2996RE
Date Sampled: 05/01/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
loil Extract Volume: (uL) ----Soil Aliquot Volume:
'
____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone . .S,o -z-:-9
71-43-2---------Benzene 1.0
75-27-4---------Bromochloromethane 1. 0
75-27-4---------Bromodichloromethane 1.0
75-25-2---------Bromoform 1.0
74-83-9---------Bromomethane 1.0
78-93-3---------2-Butanone 5.0
75-15-0---------Carbon disulfide 1.0
56-23-5---------Carbon tetrachloride 1.0
108-90-7--------Chlorobenzene 1.0
75-00-3---------Chloroethane 1.0
67-66-3---------Chloroform 1.0
74-87-3---------Chloromethane 1.0
124-48-1--------Dibromochloromethane 1.0
96-12-8---------1,2-Dibromo-3-chloropropane 1.0
106-93-4--------1,2-Dibromoethane -1.0
95-50-1---------1,2-Dichlorobenzene 1.0
541-73-1--------1,3-Dichlorobenzene 1.0
106-46-7--------1,4-Dichlorobenzene 1.0
75-34-3---------1,1-Dichloroethane 1.1
107-06-2--------1,2-Dichloroethane 1.0
75-35-4---------1,1-Dichloroethene /.Oh-5-
156-59-2--------cis-1,2-Dichloroethene 2.5
156-60-5--------trans-1,2-Dichloroethene 1.0
78-87-5---------1,2-Dichloropropane --1.0
10061-01-5------cis-1,3-Dichloropropene 1.0
10061-02-6------trans-1,3-Dichloropropene 1.0
100-41-4--------Ethylbenzene --1.0
591-78-6--------2-Hexanone 5.0
75-09-2---------Methylene chloride 3.7
108~10-1--------4-Methyl-2-pentanone 5.0
100-42-5--------Styrene 1.0
79-34-5---------1,1,2,2-Tetrachloroethane __ 1.0
FORM I VOA
Q
-t, (./
u u u u u
u u u u u u u u u
u u u u
u
i)
u
u
u u u u
u u u
I FORM 1
00128
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I W-22S
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water) WATER
lample wt/vol: 25. 00 (g/mL) ML
Level: (low/med) LOW
I Moisture: not dee.
JC Column: DB-624 ID: 0.53 (mm)
loil Extract Volume: (uL) ----
Lab Sample ID: 98002996
Lab File ID: 2996RE
Date Sampled: 05/01/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
Soil Aliquot Volume:
1 CAS NO: COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I
I
I
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene
C
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------l,l,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM l VOA
3.6
1.0 u
0.88 J
1.0 u
0.12 J
0.45 J
1.0 u
I
I
00143
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-20I *
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
_13-trix: (soil/water)
l,_mple wt/vol:
rve~: (low/med)
• Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
1
f: Column: DB-624 ID: 0.53 (mm)
!oil Extract Volume: (uL) ----
Lab Sample ID: 98002997
Lab File ID: 2997DL3
Date Sampled: 04/29/98
Date Analyzed: 05/08/98
Dilutio_n Factor: 2. O
Soil Aliquot Volume:
I
·I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone Io
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
v74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide -
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
--
10061-02-6------trans-1,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2-----·--Methylene chloride
108-10-1--

-

-

-
•· --4-Methyl-2-pentanone
100-42-5--------styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
---. -2.0
2.0
2.0
2.0
2.0
10
0.48
2.0
2.0
2.0
0.77
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
0.40
25
2.0
8.6
2.0
2.0
2.0
10
4.0
1. 4
2.0
2.0
, = RESULTS SHOULD BE CONSIDERED AS ESTIMATED. SEE CA3E NARRATIVE.
I FORM I VOA
I
Q
JD
UD
UD
UD
UD
UD
UD
JD
UD
UD
UD
JD
UD
UD
UD
UD
UD
UD
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UD
UD
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D
UD
D
UD
UD
UD
UD
UD
JD
UD
UD
✓
.J_
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I
00144
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-201 *
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
latrix: (soil/water)
'lample wt/vol :
level: (low/med)
~ Moisture: not dee.
WATER
25. 00 (g/mL) ML
LOW
IC Column: DB-<;24 ID: 0.53 (mm)
Lab Sample ID: 98002997
Lab File ID: 2997DL3
Date Sampled: 04/29/98
Date Analyzed: 05/08/98
Dilution Factor: 2.0
Soil Extract Volume: (uL) ----Soil Aliquot Volume: ____ (uL)
I
'I:
I
I
* = ,1
I
i
I -.'
I
I
I
i
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene
108-88-3--------Toluene ------
71-55-6---------1,l,l-~richloroethane
79-00-5---------1,1,2-Trichloroethane ___ _
79-01-6---------Trichloroethene -------75-01-4---------Vinyl chloride ______ _
1330-20-7-------Xylene(total) _______ _
S/0 %8'tl BE-D
2.0 UD
2.0 UD
2.0 UD
18 D
2.0 UD
2.0 UD
RESULTS SHOULD BE CONSIDERED AS ESTIMATED. SEE CASE NARRATIVE.
FORM I VOA
I ,( 1/r> q, ,
V >--"'
Y
UJ
r.J::r
v:f
T
;)£ JJ
I 00167
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-20S
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
lftrix: (soil/water)
"-mple wt/vol:
rve~: (low/med)
Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
t:. Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 98002998
Lab File ID: 2998
Date Sampled: 04/29/98
Date Analyzed: 05/07/98
Dilution Factor: 1.0
''oil Extract Volume: (uL) ----Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
i
I
I
i
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone .S.ohB-
71-43-2---------Benzene
1. 0
75-27-4---------Bromochloromethane 1.0
75-27-4---------Bromodichloromethane 1.0
75-25-2---------Bromoform 1.0
74-83-9---------Bromomethane 1.0
78-93-3---------2-Butanone
5.0
75-15-0---------Carbon disulfide 1.0
56-23-5---------Carbon tetrachloride -1.0
108-90-7---~----Chlorobenzene 1.0
75-00-3---------Chloroethane 1.0
67-66-3---------Chloroform ·0.23
74-87-3---------Chloromethane 1.0
124-48-1--------Dibromochloromethane 1.0
96-12-8---------1,2-Dibromo-3-chloropropane 1.0
106-93-4--------1,2-Dibromoethane -1.0
95-50-1---------1,2-Dichlorobenzene 1.0
541-73-1--------1,3-Dichlorobenzene 1.0
106-46-7--------1,4-Dichlorobenzene 1.0
75-34-3---------1,1-Dichloroethane
1.0
107-06-2--------1,2-Dichloroethane
1. 0
75-35-4---------1,1-Dichloroethene
1.0
156-59-2--------cis-l,2-Dichloroethene
3.4
156-60-5--------trans-l,2-Dichloroethene
1.0
78-87-5---------1,2-Dichloropropane
--0.28
10061-01-5------cis-l,3-Dichloropropene
1.0
10061-02-6------trans-l,3-Dichloropropene 1.0
100-41-4--------Ethylbenzene --1.0
591-78-6--------2-Hexanone 5.0
75-09-2---------Methylene chloride 2.0
108-10-1--------4-Methyl-2-pentanone 5.0
100-42-5-------Styrene 1.0
79-34-5---------1,1,2,2-Tetrachloroethane 1.0 --
FORM I VOA
,3-u
u u u u u u
u u
u u
J u u
u
u u u u u u u
u
J u u u u u u u u
---
I FORM 1
00168
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-20S
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
l.mple wt/vol:
lirvel: (low/med)
IMoisture: not dee.
WATER
25. 00 (g/mL) ML
LOW
I Column: DB-624 ID: 0. 53 (mm)
' il Extract Volume: (uL) • ----
. Lab Sample ID: 98002998
Lab File ID: 2998
Date Sampled: 04/29/98
Date Analyzed: 05/07/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I ,r. CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
1·
i
I
I
!'
i
I
'l
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
120-82-1--------1 2 4-Trichlorobenzene ' ' ' 71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
20
1.0 u
1.0 u
1.0 u
1.0 u
0.89 J
1.0 u
1.0 u -
I
I
Lab lb
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA
00180
CLIENT SAMPLE NO.
FB42998
SDG No.: FCX.V2991
l trix: (soil/water)
mple wt/vol:
WATER
25.00 (g/mL) ML
LOW
Lab Sample ID: 98002999
Lab File ID: 2999RE
Date Sampled: 04/29/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
,,, vel: (low/med)
Moisture: not dee.
1/'c Column: DB-624 ID: 0.53 (mm)
.:,Oil Extract Volume: (uL) ----Soil Aliquot Volume:
I'
I
I
1·
I ,,
I
I
I
I
'I
I-
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4 -

-

-

-

-

-

-

-
-Bromodi,chloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride -
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
--
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachioroethane __
FORM I VOA
1.7 J
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
2.0 u
5.0 u
1.0 u
1.0 u
____ (uL)
Q
FORM 1 I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
1f ab Code : NA Batch No. : NA SAS No.: NA
00181
CLIENT SAMPLE NO.
FB42998
SDG No.: FCX.V2991
Matrix: (soil/water)
lample wt/vol:
llf'evel: (low/med)
• & Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
9iC Column: DB-624 ID: 0.53 (mm)
'3oil Extract Volume: (uL) ----
Lab Sample ID: 98002999
Lab File ID: 2999RE
Date Sampled: 04/29/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
·1
I
·1
I
I
I
I
I
'I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene ------
71-55-6---------1,l,l-Trichloroethane
79-00-5---------1,1,2-Trichloroethane ___ _
79-01-6---------Trichloroethene -------75-01-4---------Vinyl chloride ______ _
1330-20-7-------Xylene(total) _______ _
FORM I VOA
1. 0 U
1.0 U
1.0 U
1.0U
1. 0 U
1. 0 U
1.0 U
I
I Lab Name:
lab Code:
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
ECKENFELDER INC. Contract: EL PASO ENERGY
NA Batch No. : NA SAS No.: NA
00433
CLIENT SAMPLE NO.
TRIP BLANK
#1022 & #1023
SDG No.: FCX.V2991
Matrix: (soil/water) WATER Lab Sample ID: 98003129
Lab File ID: 3129RE
Date Sampled: 05/06/98
Date Analyzed: 05/13/98
Dilution Factor: 1.0
Soil Aliquot Volume:
lample wt/vol: 25. 00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
l"C Column: DB-624 ID: 0.53 (mm)
. oil Extract Volume: (uL) ----
'I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L ,,
I
I
I
I
I
I ,,
I
I
I
I
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4 -

-

-

-

-

-

-

-
-Bromodichloro,methane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride -
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
2.5 J
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
5.0 u
1.0 u
1 .. 0 u
1. 0 u
1.0 u
1.0 u
1. 0 u
1. 0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
0.31 J
5.0 u
1.0 u
1.0 u
00434 I
I
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
TRIP BLANK
#1022 & #1023
Lab Name: ECKENFELDER.INC. Contract: EL PASO ENERGY
lb Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
lmple wt/vol:
·leve~: (low/med)
Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
I Column: DB-624 ID: 0.53 (mm)
il Extract Volume: (uL) ----
Lab Sample ID: 98003129
Lab File ID: 3129RE
Date Sampled: 05/06/98
Date Analyzed: 05/13/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
-1
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I
I
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene
108-88-3------~-Toluene
71-55-6--

-

-

-

-

-
~-1, 1, 1-T,richloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---~-----Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
-
I
I
Lab Name:
lab Code:
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
ECKENFELDER INC. Contract: EL PASO ENERGY
NA Batch No. : NA SAS No.: NA
00184
CLIENT SAMPLE NO.
TRIP BLANK
#1021 & #1022
SDG No.: FCX.V2991
Matrix: (soil/water) WATER Lab Sample ID: 98003000
lample wt/vol: 25.00 (g/mL) ML Lab File ID: 3000RE
Level: (low/med) LOW
I Moisture: not dee.
jC Colu~n: DB-624 ID: 0.53 (mm)
loil Extract Volume: (uL) ----
Date Sampled: 04/30/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I ,,
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromod{chloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride -
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-1,2-Dichloroethene
156-60-5--------trans-1,2-Dichloroethene
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-1,3-Dichloropropene
--
10061-02-6------trans-1,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
2.3 J
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1-.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
5.0 u
2.0 u
5.0 u
1.0 u
1. 0 u
00185
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
TRIP BLANK
#1021 & #1022
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lb Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
fmple wt/vol:
Level: (low/med)
IMoisture: not dee.
WATER
25.00 (g/mL) ML
LOW
GC ColumD: DB-624 ID: 0.53 (mm)
lil Extract Volume: (uL) ----
Lab Sample ID: 98003000
Lab File ID: 3000RE
Date Sampled: 04/30/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6--~------l,l,l-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
I
lab
00190 FORM 1 CLIENT SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
W-5S * Name: ECKENFELDER INC. Contract: EL PASO ENERGY
[
b ~ode: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
trix: (soil/water) WATER
wt/vol:
(low/med) I Moisture: not dee.
25.00
LOW
(g/mL) ML
GC Column: DB-624 ID: 0. 53 (mm)
Lab Sample ID: 98003001
Lab File ID:
Date Sampled:
3001DL2
04/30/98
Date Analyzed: 05/08/98
Dilutin.n Factor: 5.0 loil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride -108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
6 7 - 6 6 -3 ---•------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
61
2.9
5.0
5.0
5.0
5.0
25
5.0
5.0
5.0
5.0
2.2
5.0
5.0
5.0
5.0
5.0
5.0
5.0 75-34-3---------1,1-Dichloroethane :sfo 34% 107-06-2--------1,2-Dichloroethane 3.8 75-35-4---------1,1-Dichloroethene 83 156-59-2--------cis-1,2-Dichloroethene I SC'O Hil'O' 156-60-5--------trans-1,2-Dichloroethene 3.1 --78-87-5---------1,2-Dichloropropane 2.4 10061-01-5------cis-1,3-Dichloropropene 5.0 10061-02-6------trans-1;3-Dichloropropene 5.0 100-41-4--------Ethylbenzene --5.0 591-78-6--------2-Hexanone 25 75-09-2---------Methylene chloride 3.4 108-10-1--------4-Methyl-2-pentanone 25 100-42-5--------Styrene 5.0 79-34-5---------1,1,2,2-Tetrachloroethane 5.0 --I= RESULTS SHOULD BE CONSIDERED AS ESTIMATED. SEE CASE NARRATIVE.
I
I
FORM I VOA
Q
D u -J
JD T
UD VJ .J
UD
UD
UD
UD
UD
UD
UD ,,.
UD u I JD .J
UD (.;J
UD
I UD
UD
UD I UD
UD ~ i:J'e D J
JD .T D .T PED w JD 1-J JD
~'J UD
UD 1 UD
UD
JD J
UD V:T
UD 1 UD
00191
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-5S *
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
.b ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V2991
!f~trix: (soil/water) WATER
,tmple wt/vol:
Level: (low/med)
1, Moisture: not dee_.
25. 00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0. 53 (mm)
Jil Extract Volume: ____ (uL)
Lab Sample ID: 98003001
Lab File ID: 3001DL2
Date Sampled: 04/30/98
Date Analyzed: 05/08/98
Dilution Factor: 5.0
Soil Aliquot Volume:
I
I
I
I=
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene .,;;ldo z-frO -BE D
108-88-3--------Toluene 5.0 .UD
71-55-6---------1,1,1-Trichloroethane /-1/0 ~ -BE.P
79-00-5---------1,1,2-Trichloroethane 13 D
79-01-6---------Trichloroethene 55 D
75-01-4---------Vinyl chloride 8.2 D
1330-20-7-------Xylene(total) 5.0 UD
,
RESULTS SHOULD BE CONSIDERED AS ESTIMATED. SEE CASE NARRATIVE.
FOFu'-1 I VOA
I
T'
i) . T :r
I 00222
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
'ab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
W-24S
tab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water) WATER tample wt/vol:
Level: (low/med) I Moisture: not dee.
25. 00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 98003002
Lab File ID: 3002RE
Date Sampled: 05/01/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0 loil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
'
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone __________ _
71-43-2---------Benzene...---~-------75-27-4---------Bromochloromethane 75-27-4---------Bromodi.chlorometha_n_e ___ _
75-25-2---------Bromoform 74-83-9---------Bromometh_a_n_e ________ _
78-93-3---------2-Butanone~~~-------
75-15-0---------Carbon disulfide 56-23-5---------Carbon tetrachlo_r_i~a-e ___ _
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane --------
67-66-3---------Chloroform 74-87-3---------Chlorometh_a_n_e _______ _
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chlorop-ro-p-an_e_
106-93-4--------1,2-Dibromoetha~e -
95-50-1---------1,2-Dichlorobenzene ____ _
541-73-1--------1,3-Dichlorobenzene 106-46-7--------1,4-Dichlorobenzene ____ _
75-34-3---------1,1-Dichloroethane ____ _
107-06-2--------1,2-Dichloroethane ____ _
75-35-4---------1,1-Dichloroethene 156-59-2--------cis-l,2-Dichloroet_h_e_n_e __ _
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------l,2-Dichloropropane ___ -_-_-_-
10061-01-5------cis-l,3-Dichloropropene __ _
10061-02-6------trans-l,3-Dichloropropene
100-41·-4--0 -----Ethylbenzene _______ -:::_-:::_=
591-78-6--------2-Hexanone 75-09-2---------Methylene_c_n~l-o_r_i_d_e _____ _
108-10-1--------4-Methyl-2-pentanone ----100-42-5--------Styrene ___ ~~--~---
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
.s:o.l.-2--a
1.0U
1.0U
1. 0 U
1.0 U
1. 0 U
5. 0 U
1.0 U
1. 0 U
1.0U
1.0 U
1.0U
1. 0 U
1.0 U
1.0U
1.0 U
1. 0 U
1. 0 U
1.0U
1.0 U
1.0U
1. 0 U
1. 0 U
1. 0 U
1.0U
1. 0 U
1.0 U
1. 0 U
5. 0 U
2. 0 U
5. 0 U
l.0U
1.0 U
Q /1 ··/qf' I '.) Di--lc
u
00223
FORM l CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-24S
Name: ECKENFELDER.INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water) WATER
lample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
GC Column: DB-624· ID: 0.53 (mm)
loil Extract Volume : ____ (uL)
Lab Sample ID: 98003002
Lab File ID: 3002RE
Date Sampled: 05/01/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
u
0
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene 0.35 J
108-88-3--------Toluene 1.0 u
71-55-6---------1,l,l-Trichloroethane 1.0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 1.0 u
75-01-4---------Vinyl chloride 1.0 u
1330-20-7-------Xylene(total) 1.0 u
-
FORM I VOA
I
lab
00230
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-20S DUPE
Name: ECKENFELDER.INC. Contract: EL PASO ENERGY
.ab ~ode: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
lllatrix: (soil/water) WATER
'ample
Level:
wt/vol:
(low/med)
.f Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.133 (mm)
Lab Sample ID: 98003003
Lab File ID:
Date Sampled:
3003RE
04/29/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
loil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone S.o..;i..,..g
71-43-2---------Benzene 1.0
75-27-4---------Bromochloromethane 1.0
75-27-4---------Bromodfchloromethane 1.0
75-25-2---------Bromoform 1.0
74-83-9---------Bromomethane 1. 0
78-93-3---------2-Butanone 5.0
75-15-0---------Carbon disulfide 1.0
56-23-5---------Carbon tetrachloride -1. 0
108-90-7--------Chlorobenzene 1.0
75-00-3---------Chloroethane 1.0
67-66-3---------Chloroform 0.21
74-87-3---------Chloromethane 1..0
124-48-1--------Dibromochloromethane 1.0
96-12-8---------1,2-Dibromo-3-chloropropane 1.0
106-93-4-------0 1,2-Dibromoethane -1. 0
95-50-1---------1,2-Dichlorobenzene 1.0
541-73-1--------1,3-Dichlorobenzene 1.0
106-46-7--------1,4-Dichlorobenzene 1.0
75-34-3---------1,1-Dichloroethane 1.0
107-06-2--------1,2-Dichloroethane 1.0
75-35-4---------1,1-Dichloroethene 1.0
156-59-2--------cis-1,2-Dichloroethene 3.1
156-60-5--------trans-1,2-Dichloroethene 1. 0
78-87-5---------1,2-Dichloropropane --0.26
10061-01-5------cis-1,3-Dichloropropene 1. 0
10061-02-6------trans-1,3-Dichloropropene 1. 0
100-41-4--------Ethylbenzene --1.0
591-78-6--------2-Hexanone 5.0
75-09-2---------Methylene chloride 2.0
108-10-1--------4-Methyl-2-pentanone 5.0
100-42-5--------Styrene 1.0
79-34-5---------1,1,2,2-Tetrachloroethane 1.0 --
FORM I VOA
Q
-a u
u u u u
u u
u u u u
J
u
u u u
u
u
u
u
u u
u
J
u u u
u u
u u
u
00231
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-20S DUPE
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Batch No. : NA tb Code: NA
Matrix: (soil/water)
tmple wt/vol:
SAS No.: NA SDG No.: FCX.V2991
WATER
25. 00 (g/mL) ML
Level: (low/med) LOW
I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 98003003
Lab File ID: 3003RE
Date Sampled: 04/29/98.
Date Analyzed: 05/12/98
Dilution Factor: 1.0
Lil Extract Volume : ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
0
m
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q 1/15/11-w
127-18-4--------Tetrachloroethene 17
108-88-3--------Toluene 1. 0 u
71-55-6---------1,1,1-Trichloroethane 1.0 u
79-00-5--

-

-

-

-

-

-
-1, 1, 2·-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 0.80 J
75-01-4---------Vinyl chloride 1.0 u
1330-20-7-------Xylene(total) 1.0 u
FORM I VOA
00242
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EB42998
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
tab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water) WATER Lab Sample ID: 98003004
lsample wt/vol: 25.00 (g/mL) ML Lab File ID: 3004RE
Level: (low/med) LOW
1% Moisture: not dee.
Date Sampled: 04/29/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
Soil Aliquot Volume:
GC Column: DB-624 ID: 0.53 (mm)
lsoil Extract Volume: ____ (uL)
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I
I
I
I
I
•
I
B
I
67-64-1---------A~etone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride -
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethani
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethyl.benzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
3.1 J
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
5.0 u
1.0 u
1. 0 u
1. 0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1. 0 u
1. 0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
2.0 u
5.0 u
1.0 u
1.0 u
I FORM 1
00243
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EB42998 lb Name: ECKENFELDER INC. Contract: EL PASO ENERGY
l b ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V2991
trix: (soil/water) WATER
fmple wt/vol:
Level: (low/med)
IMoisture: not dee.
GC Column: DB-624
25. 00 (q-/mL) ML
LOW
ID: 0.53 (mm)
lil Extract Volume: ____ (uL)
Lab Sample ID: 98003004
Lab File ID: 3004RE
Date Sampled: 04/29/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I CAS NO. COMPOUND.
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I
I
I
I
I
B
u
I
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
00247
CLIENT SAMPLE NO.
W-22I
-tb Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
t-mple wt/vol:
WATER Lab Sample ID: 98003005
25.00 (g/mL) ML Lab File ID: 3005RE
Level: (low/med) LOW Date Sampled: 05/01/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I Moisture: not dee.
GC Column: DB-624 ID: 0. 53 (mm)
loil Extract Volume: ____ (uL)
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodi'chloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane
--
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
5.0
0.28
1.0
1.0
1.0
1. 0
5.0
1.0 -1.0
1.0
1.0
0.54
1.0
1.0
1.0
1. 0
1.0
1. 0
1. 0
4G· 45
1. 0
20
100-±-0-0
0.46
1.0
1.0
1.0
1.0
5.0
2.0
5.0
1. 0
1. 0
u
J u u u u
u
u u u u
J u u u u u u u
E--D u
-B j)
J
u u u u u
u u u
u
00248
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-22I
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
[
b ~ode: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
trix: (soil/water) WATER
tmple
Level:
wt/vol:
(low/med)
I Moisture: not dee.
25. 00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
(,i1 Extract Volume: (uL) ----
Lab Sample ID: 98003005
Lab File ID:
· Date Sampled:
3005RE
05/01/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
m
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
____ (uL)
1 11sh'ff, ;, {:>t-.W Q
127-18-4--------Tetrachloroethene /°5::> -r5-& i!:" .D
108-88-3--------Toluene 1.0 u
71-55-6---------1,1,1-Trichloroethane 11
79-00-5---------1,1,2-Trichloroethane 0.31 J
79-01-6---------Trichloroethene 11
75-01-4---------Vinyl chloride 2.1
1330-20-7-------Xylene(total) 1.0 u
-
FORM I VOA
I
I 00330
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
PURGE WATER*
ECKENFELDER INC . Contract: EL PASO ENERGY
.. b ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V2991
'atrix: (soil/water) WATER
tmple wt/vol:
Level: (low/med)
I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Jil Extract Volume: ____ (uL)
Lab Sample ID: 98003120
Lab File ID: 3120
Date Sampled: 05/06/98
Date Analyzed: 05/08/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone s·. c'J½-:-5
71-43-2---------Benzene 0.11
75-27-4---------Bromochloromethane 1.0
75-27-4---------Bromodfchloromethane 1. 0
75-25-2---------Bromoform 1.0
74-83-9---------Bromomethane 1.0
78-93-3---------2-Butanone 3.2
75-15-0---------Carbon disulfide 1.0
56-23-5---------Carbon tetrachloride -1.0
108-90-7--------Chlorobenzene 1.0
75-00-3---------Chloroethane 0.12
67-66-3---------Chloroform 0.90
74-87-3---------Chloromethane 1.0
124-48-1--------Dibromochloromethane 1.0
96-12-8---------1,2-Dibromo-3-chloropropane 1.0
106-93-4--------1,2-Dibromoethane -1.0
95-50-1---------1,2-Dichlorobenzene 1. 0
541-73-1--------1,3-Dichlorobenzene 1. 0
106-46-7--------1,4-Dichlorobenzene I. 0
75-34-3---------1,1-Dichloroethane 1.0
107-06-2--------1,2-Dichloroethane 0.32
75-35-4---------1,1-Dichloroethene 2.1
156-59-2--------cis-l,2-Dichloroethene 4.6
156-60-5--------trans-l,2-Dichloroethene 1. 0
78-87-5---------1,2-Dichloropro: --0.60 ,me
10061-01-5------cis-l,3-Dichloropropene 1.0
10061-02-6------trans-l,3-Dichloropropene 1.0
100-41-4--------Ethylbenzene --1. 0
591-78-6--------2-Hexanone 5.0
75-09-2---------Methylene chloride 2.0
108-10-1--------4-Methyl-2-pentanone 5.0
100-42-5--------Styrene 1.0
79-34-5---------1,1,2,2-Tetrachloroethane __ 1.0
RESULTS SHOULD BE CONSIDERED AS ESTIMATED. SEE CASE NARRATIVE.
FORM I VOA
·a-
J u u
u u
J u
u
u
J
J
u
u
u
u u
u u u
J
u
J
u
u
u
u
u
u
u
u
(./ -~
'J
~
.J
U✓
UJ
1 U, --J
T J y
-17
J T ~
.)
:J.J :r
JI'
~-
00331
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
PURGE WATER*
Name: ECKENFELDER.INC. Contract: EL PASO ENERGY
tb Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
tmple wt/vol:
Level: (low/med)
I M~isture: X:ot dee.
WATER
25. 00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0;53 (mm)
l,il Extract Volume: ____ (uL)
Lab Sample ID: 98003120
Lab File ID: 3120
Date Sampled: 05/06/98
Date Analyzed: 05/08/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene /.lO ~
108-88-3--------Toluene 0 " ,.., .... I,
71-55-6---------1 1 1-Trichloroethane 1.0 ' , ' 79-00-5---------1,1,2-Trichloroethane 1. 0
79-01-6---------Trichloroethene 10
75-01-4---------Vinyl chloride 1.0
1330-20-7-------Xylene(total) 1. 0
-
RESULTS SHOULD BE CONSIDERED AS ESTIMATED. SEE CASE NARRATIVE.
FORM I VOA
F:..D ~ -u u
u u
J
-:t°"
\JJ
u:r :r
J
J
00278
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-29I
Name: ECKENFELDER INC. Contract: EL PASO ENERGY rb Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
tmple wt/vol:
Level: (low/med) I Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 98003006
Lab File ID: 3006DRE1
Date Sampled: 05/01/98
Date Analyzed: 05/12/98
Dilution Factor: 2.5 loil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone I ;l.. -. ~
71-43-2---------Benzene 2.5
75-27-4---------Bromochloromethane 2.5
75-27-4---------Bromodichloromethane 2.5
75-25-2---------Bromoform 2.5
74-83-9---------Bromomethane 2.5
78-93-3---------2-Butanone 12
75-15-0---------Carbon disulb.de 2.5
56-23-5---------Carbon tetrachloride -2.5
108-90-7--------Chlorobenzene 2.5
75-00-3---------Chloroethane 2.5
67-66-3---------Chloroform 1.1
74-87-3---------Chloromethane 2.5
124-48-1--------Dibromochloromethane 2.5
96-12-8---------l,2-Dibromo-3~chloropropane 2.5
106-93-4--------1,2-Dibromoethane -2.5
95-50-1---------1,2-Dichlorobenzene 2.5
541-73-1--------1,3-Dichlorobenzene 2.5
106-46-7--------1,4-Dichlorobenzene 2.5
75-34-3---------1,1-Dichloroethane 5.4
107-06-2--------1,2-Dichloroethane 2.5
75-35-4---------1,1-Dichloroethene 4.4
156-59-2--------cis-l,2-Dichloroethene 8.0
156-60-5--------trans-l,2-Dichloroethene 2.5
78-87-5---------1,2-Dichloropropane --2.5
10061-01-5------cis-l,3-Dichloropropene 2.5
10061-02-6------trans-l,3-Dichloropropene 2.5
100-41-4--------Ethylbenzene --2.5
591-78-6--------2-Hexanone 12
75-09-2---------Methylene cnloride 5.0
108-10-1--------4-Methyl-2-pentanone 12
100-42-5--------Styrene 2.5
79-34-5---------1,1,2,2-Tetrachloroethane __ 2.5
FORM I VOA
Q
---j) (,I
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
JD
UD
UD
UD
UD
UD
UD
UD
D
UD
D
D
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
00279 I
lab
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-29I
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
1ab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V2991
"1atrix: (soil/water) WATER Lab Sample ID: 98003006
tampl_e
Level:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
Lab File ID:
Date Sampled:
3006DRE1
05/01/98
I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Date Analyzed: 05/12/98
Dilution Factor: 2.5
loil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
127-18-4--------Tetrachloroethene
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-88-3--------Toluene · ------
71-55-6---------1, 1, 1-T.richloroethane
79-00-5---------1,1,2-Trichloroethane ___ _
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride-------
1330-20-7-------Xylene(total) _______ _
FORM I VOA
42 D
2.5 UD
2.5 UD
2.5 UD
1.4 JD
2.5 UD
2.5 UD
Q
00293 I
lab
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELDER.INC. Contract: EL PASO ENERGY
HOLDING
BLANK 050698
fab ~ode: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
'1atrix: (soil/water) WATER Lab Sample ID: 98003061
'ample
Level:
wt/vol:
(low/med)
25.00 (g/rnL) ML
LOW
Lab File ID:
Date Sampled:
3061RE
05/06/98
I Moisture: not dee.
GC Column: DB-624 ID: 0. 53 (mm)
loil Extract Volume: ____ (uL)
Date Analyzed: 05/12/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromod{chloromethane
75-25-2---------Bromoforrn
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15°0---------Carbon disulfide
56-23-5---------Carbon tetrachloride -
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroforrn
74-87-3---------Chloromethane
i24-48-l--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1-------~-l,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pent ·none
100-42-5--------Styrene
79-34-5--

-

-

-
----1, 1, 2, 2-Tet::adiloroethane --
FORM I VOA
2.5 J
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
5.0 u
1. 0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
.1. 0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1. 0 u
1. 0 u
1.0 u
1.0 u
1.0 u
5.0 u
0.22 J
5.0 u
1.0 u
1. 0 u
00294
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
HOLDING
BLANK 050698
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
[
b ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V2991
trix: (soil/water) WATER
tmple
Level:
wt/vol:
(low/med)
I Moisture: not dee.
25. 00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Extract Volume: ____ (uL)
Lab Sample ID: 98003061
Lab File ID:
Date Sampled:
3061RE
05/06/98
Date Analyzed: 05/12/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene 1.0 u
108-88-3--------Toluene 1.0 u
71-55-6---------1,1,1-Trichloroethane 1.0 u
79-00-5---------1,1,2-Trichloroethane 1. 0 u
79-01-6---------Trichloroethene 1.0 u
75-01-4---------Vinyl chloride 1. 0 u
1330-20-7-------Xylene(total) 1. 0 u
FORM I VOA
00299
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-9S
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Batch No.: NA tb Code: NA
Matrix: (soil/water)
tmple wt/vol:
SAS No.: NA SDG No.: FCX.V2991
Lab Sample ID: 98003118
Lab File ID: 3118RED1
Date Sampled: 05/05/98
Date Analyzed: 05/13/98
Dilution Factor: 10.0
Level: (low/med)
I Moisture: not dee.
WATER
25. 00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
loil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodi~hloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulb.de
56-23-5---------Carbon tetrachlon.de -
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroetnene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene cnlon.ae
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachl~roethane --
F".,RM I VOA
50 UD
10 UD
10 UD
10 UD
10 UD
10 UD
50 UD
10 UD
10 UD
10 UD
10 UD
2.1 JD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
1. 9 JD
10 UD
10 UD
10 UD
10 UD
10 UD
50 UD
20 UD
50 UD
10 UD
10 UD
I
I
00300
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-9S
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
lamp le wt/vol:
11/t'evel: (low/med)
I. Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
a,c Column: DB-624 ID: O. 53 (mm)
Lab Sample ID: 98003118
Lab File ID: 3118RED1
Date Sampled: 05/05/98
Date Analyzed: 05/13/98
Dilution Factor: 10.0
~oil Extract Volume: (uL) ----Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene 5/CCn:tHl
108-88-3--------Toluene 10
71-55-6---------1 1 1-Trichloroethane ' ' . 10
79-00-5---------1,1,2-Trichloroethane 10
79-01-6---------Trichloroethene 14
75-01-4---------Vinyl chloride 10
1330-20-7-------Xylene(total) 10
-
FORM I VOA
Q
-9&D
UD
UD
UD
D
UD
UD
l/13/cl<
J:)1-4-
I 00314
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I W-9S DUPE
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lb Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
lmple wt/vol:
WATER
25. 00 (g/mL) ML
LOW
Lab Sample ID: 98003119
Lab File ID: 3119RED1
Date Sampled: 05/05/98
Date Analyzed: 05/13/98
Dilution Factor: 10.0
Soil Aliquot Volume:
iivel: (low/med)
IMoisture: not dee.
I Column: DB-624 ID: 0.53 (mm)
il Extract Volume: (uL) ----
CONCENTRATION UNITS: ( I-CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
I
I
I
I
I
I
I
I
I
I
I
I
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulb.de
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroforrn
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02~6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene cnloride
108-10-1--------4-Methyl-2-pentanone
100-42-~--------Styrene
79-34-5 --------1,1,2,2-Tetrachloroethane --
FORM I VOA
5c-tt .J!J"
10 UD
10 UD
10 UD
10 UD
10 UD so UD
10 UD -10 UD
10 UD
10 UD
2.2 JD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
2.0 JD
10 UD
10 UD
10 UD
10 UD
10 UD so UD
20 UD so UD
10 UD
10 UD
D
I FORM 1
00315
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I W-9S DUPE
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water) WATER
lample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
life Column: DB-624 ID: 0.53 (mm)
lloil Extract Volume: (uL) ----
Lab Sample ID: 98003119
Lab File ID: 3119RED1
Date Sampled: 05/05/98
Date Analyzed: 05/13/98
Dilution Factor: 10.0
Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
E
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene :;? .;?,:JO ..;H-9-0 DE-Z>
108-88-3--------Toluene 10 UD
71-55-6---------1,1,1-Trichloroethane 10 UD
79-00-5---------1,1,2-Trichloroethane 10 UD
79-01-6---------Trichloroethene 13 D
75-01-4---------Vinyl chloride 10 UD
1330-20-7-------Xylene(total) 10 UD
FORM I VOA
00357
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-28I
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
lample wt/vol:
WATER Lab Sample ID: 98003121
25. 00 (g/mL) ML Lab File ID: 3121RED1
Level: (low/med) LOW
I Moisture: not dee.
Ire Column: DB-624 ID: 0.53 (mm)
· oil Extract Volume: (uL) ----
Date Sampled: 05/05/98
Date Analyzed: 05/13/98
Dilution Factor: 10.0
Soil Aliquot Volume:
CONCENTRATION UNITS: I CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
I
I
' I
I
I
I
I
I
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4 -

-

-

-

-

-

-

-
-Bromodi.chloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disull:icle
56-23-5---------Carbon tetrachloricle
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,·1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
110061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloricle
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
50 UD
10 UD
10 UD
10 UD
10 UD
10 UD
50 UD
10 UD -10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
2.9 JD
16 D
10 UD
10 UD
10 UD
10 UD
10 UD
50 UD
20 UD
50 UD
10 UD
10 UD
I FORM 1
00358
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-28I
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water) WATER
,lample wt/vol: 25. 00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
l·eoc Column: DB-624 ID: 0.53 (mm)
oil Extract Volume: (uL) ----
Lab Sample ID: 98003121
Lab File ID: 3121RED1
Date Sampled: 05/05/98
Date Analyzed: 05/13/98
Dilution Factor: 10.0
Soil Aliquot Volume:
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene 170 D
108-88-3--------Toluene 10 UD
71-55-6---------1,1,1-Trichloroethane 10 UD
79-00-5---------1,1,2-Trichloroethane 10 UD
79-01-6---------Trichloroethene 42 D
75-01-4---------Vinyl chloride 10 UD
1330-20-7-------Xylene(total) 10 UD
FORM I VOA
I
00378
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-19S
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
[
. trix: ( soil/water)
· mple wt/vol:
WATER
25. 00 (g/mL) ML
LOW
Lab Sample ID: 98003122
Lab File ID: 3122DUP
Date Sampled: 05/05/98
Date Analyzed: 05/11/98
Dilution Factor: 2.5
,rT vel: (low/med)
Moisture: not dee . . f Column: DB-624 ID: 0.53 (mm)
~oil Extract Volume: (uL) Soil Aliquot Volume: ____ (uL)
11,
I
I
I
'I
,m
ff:
B
0
,D
I'
i
·1·
----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-l--------0 Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride -
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane -
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7------~-l,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-~,3-Dichloropropene
.10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
Q
12 UD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
12 UD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
0.56 JD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
0.82 JD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
2.5 UD
12 UD
5.0 UD
12 UD
2.5 UD
2.5 UD
I
I
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
00379
CLIENT SAMPLE NO.
W-19S
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
'tb Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
lmple wt/vol:
' ' ' '
(low/med) level:
Moisture: not dee.
WATER
25. 00 (g/mL) ML
LOW
jC Column: DB-624 ID: 0.53 (mm)
foil Extract Volume: (uL) ----
Lab Sample ID: 98003122
Lab File ID: 3122DUP
Date Sampled: 05/05/98
Date Analyzed: 05/11/98
Dilution Factor: 2.5
Soil Aliquot Volume: ____ (uL)
I
i
I
1i
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I
, .. ,. :1
I
I
I
·I·
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
26 D
2.5 UD
2.5 UD
2.5 UD
1.2 JD
2.5 UD
2.5 UD
I
I
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA
00386
CLIENT SAMPLE NO.
W-5I
SDG No.: FCX.V2991
Matrix: (soil/water)
lmple wt/vol:
WATER
25.00 (g/mL) ML
LOW
Lab Sample ID: 98003123
Lab File ID: 3123DL2
Date Sampled: 05/05/98
Date Analyzed: 05/11/98
·f· ve~: (low/med)
Moisture: not dee.
ac Column: DB-624 ID: 0.53 (mm) Dilution Factor: 5.0
!oil Extract Volume: (uL) ----Soil Aliquot Volume:
I
Ii
I
I
I
' I .,
I
i
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4--------~Bromochloromethane
75-27~4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride -
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
--
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VO.1
J.S :te-
5.0
5.0
5.0
5.0
5.0
25
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
3.3
5.0
3.6
4.0
5.0
5.0
5.0
5.0
5.0
25
10
25
5.0
5.0
____ (uL)
Q
~j)
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
JD
UD
JD
JD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
00387 I
I
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-5I
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
ri Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
lmple wt/vol:
11rel: (low/med)
.Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
ct Column: DB-624 ID: 0. 53 (mm)
~il Extract Volume: (uL) ----
Lab Sample ID: 98003123
Lab File ID: 3123DL2
Date Sampled: 05/05/98
Date Analyzed: 05/11/98
Dilution Factor: 5.0
Soil Aliquot Volume: ____ (uL)
1 CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I
II
I
I
I
.-·-
I
I
' ' I'
I
I
127-18-4--------Tetrachloroethene 49 D
108-88-3--------Toluene 5.0 UD
71-55-6---------1,1,1-Trichloroethane 5.0 UD
79-00-5---------1,1,2-Trichloroethane 5.0 UD
79-01-6---------Trichloroethene 4.9 JD
75-01-4---------Vinyl chloride 5.0 UD
1330-20-7-------Xylene(total) 5.0 UD
FORM I VOA
·00397
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-17S
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
tb Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
lample wt/vol:
Level: (low/med) I Moisture: not dee.
WATER
25. 00 (g/mL) ML
LOW
,fjC Column: DB-624 ID: 0.53 (mm)
loil Extract Volume: (uL)
Lab Sample ID: 98003126
Lab File ID: 3126RED1
Date Sampled: 05/05/98
Date Analyzed: 05/13/98
Dilution Factor: 250.0
Soil Aliquot Volume: ----
CONCENTRATION UNITS: I· CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
I
I
I
I
I
I
I
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodi~hloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulb.de
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5~-------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
--
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
1200 UD
250 UD
250 UD
250 UD
250 UD
250 UD
1200 UD
250 UD -250 UD
250 UD
250 UD
110 JD
250 UD
250 UD
250 UD
250 UD
250 UD
250 UD
250 UD
250 UD
250 UD
250 UD
720 D
250 UD
57 JD
250 UD
250 UD
250 UD
1200 UD
-.:,oo-g.;, cffi D
1200 UD
250 UD
250 UD
J
I
I
00398
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-17S
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water) WATER
lample wt/vol: 25.00 (g/mL) ML'
revel: (low/med) LOW I Moisture: not dee.
jC Column: DB-624 ID: 0.53 (mm)
1oil Extract Volume: (uL)
Lab Sample ID: 98003126
Lab File ID: 3126RED1
Date Sampled: 05/05/98
Date Analyzed: 05/13/98
Dilution Factor: 250.0
Soil Aliquot Volume: --------
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene r4 oco
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
Q
84000 -BB D
250 UD
250 UD
250 UD
410 D
250 UD
250 UD
(uL)
m
I
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA
00419
CLIENT SAMPLE NO.
FB5598
SDG No.: FCX.V2991
l trix: ( soil/water)
mple wt/vol:
WATER
25.00 (g/mL) ML
LOW
Lab Sample ID: 98003127
Lab File ID: 3127RE
Date Sampled: 05/05/98
Date Analyzed: 05/13/98
Dilution Factor: 1.0
Soil Aliquot Volume:
rve~: (low/med)
"Moisture: not dee.
I. Column: DB-624 ID: 0.53 (mm)
il Extract Volume: (uL) ----
1 ,, CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I
I
I
I
I
I
I
67-64-la--------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodfchloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride -
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-1,2-Dichloroethene
156-60-5--------trans-1,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-1,3-Dichloropropene
10061-02-6------trans-1,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5--·· ------1, 1, 2, 2-Tetrachloroetharcc_
FORM I VOA
3.5 J
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
5.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
0.38 J
5.0 u
1.0 u
1.0 u
I
R
00420
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
FB5598
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
lample wt/vol:
llievel: (low/med)
I Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
Lab Sample ID: 98003127
Lab File ID: 3127RE
Date Sampled: 05/05/98
Date Analyzed: 05/13/98
Dilution Factor: 1.0 •C.Column: DB-624 ID: 0.53 (mm)
~oil Extract Volume: (uL) ----Soil Aliquot Volume: ___ (uL)
I
I
I
I
I
I:
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1 1 1-Trichloroethane ' ' ' 79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
-
FORM I VOA
Q 1 \ \) \ '~i.\,~
1.0 u
0.21 J
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
fl
I
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
00426
CLIENT SAMPLE NO.
EB5598
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lb Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
lmple wt/vol:
WATER
25. 00 (g/mL) ML
LOW
Lab Sample ID: 98003128
Lab File ID: 3128RE
Date Sampled: 05/05/98
Date Analyzed: 05/13/98
Dilution Factor: 1.0
Soil Aliquot Volume:
•vel: (low/med)
IMoisture: not dee.
I. Column: DB-624 ID: 0. 53 (mm)
il Extract Volume: (uL) ----
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---~-----Carbon tetrachloride -
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-1,2-Dichloroethene
156-60-5--------trans-1,2-Dichloroethene
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-1,3-Dichl6ropropene
--
10061-02-6------trans-1,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone '
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
2.8 J
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
0.37 J
5.0 u
:i..O u
1.0 u
I
I
Lab
lab
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA
00427
CLIENT SAMPLE NO.
EB5598
SDG No.: FCX.V2991
Matrix: (soil/water)
lample wt/vol:
WATER
25.00 (g/mL) ML
LOW
Lab Sample ID: 98003128
Lab File ID: 3128RE
Date Sampled: 05/05/98
Date Analyzed: 05/13/98
Dilution Factor: 1.0
Soil Aliquot Volume:
111 evel: (low/med)
I Moisture: not dee.
1jC Column: DB-624 ID: 0.53 (mm)
loil Extract Volume: (uL) ----
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I
I
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene ------
71-55-6---------1,1,l-Trichloroethane
79-00-5---------1,1,2-Tiichloroethane ___ _
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride-------
1330-20-7-------Xylene(total) --------
FORM I VOA
1. 0 U
0.19 J
1. 0 U
1.0U
1. 0 U
1.0 U
1. 0 U
I
I
FORM 1
00440
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET HOLDING
BLANK 050798 *
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
fb Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
Jmple wt/vol:
_.eve~: (low/med)
!Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
jC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 98003130
Lab File ID: 3130
Date Sampled: 05/07/98
Date Analyzed: 05/08/98
Dilution Factor: 1.0
loil Extract Volume: (uL) ----Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I* =
I
I'
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1-------~-Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodi~hloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride -
108-90-7--~-----Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3------~--l,l-Dichloroethane
107-06-2--------1,2-Dichloroethane -
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane
--
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene · --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------S:yrene
79-34-5---------1,1,2,2-Tetrachloroethane __
0.75
1.0
1.0
1.0
1.0
1.0
5.0
1. 0
1.0
1.0
1.0
1.0
1.0
1. 0
1.0
1.0
1. 0
1. 0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
2.0
5.0
1.0
1. 0
RESULTS SHOULD BE CONSIDERED AS ESTIMATED. SEE CASE NARRATIVE.
FORM I VOA
-1J 15)1 f . Q / I ' / j)),. t'l;
J T u i.JJ u u u
u u u u u u u u
u
u
u
u
u
u u
u
u u
u u u
u
u
u
u
u
u I u -q
" '
00441
FORM 1 CLIENT SAMPLE NO. I
I
VOLATILE ORG~.NICS ANALYSIS DATA SHEET
HOLDING
BLANK 050798 *
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
la;:) Code : NA Batch No. : NA SAS No.: NA SDG No.: FCX.V2991
Matrix: (soil/water)
lample wt/vol:
~evel: (low/med)
I Moisture: not dee.
WATER
25. 00 (g/mL) ML
LOW
,We Column: DB-624 ID: 0. 53 (mm)
loil Extract Volume: (uL) ----
Lab Sample ID: 98003130
Lab File ID: 3130
Date Sampled: 05/07/98
Date Analyzed: 05/08/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L I •/1< o,
Q .1 /J.
I
I
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene 1.0
108-88-3--------Toluene 1.0
71-55-6---------1,1,1-Trichloroethane 1.0
79-00-5---------1,1,2-Trichloroethane 1.0
79-01-6---------Trichloroethene 1.0
75-01-4---------Vinyl chloride ' 1.0
1330-20-7-------Xylene(total) 1. 0
-
RESULTS SHOULD BE CONSIDERED AS ESTIMATED. SEE CASE NARRATIVE.
FORM I VOA
u uT
u
u
u u
u
u
I
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
lb Name: ECKENFELDER INC. Contract: El Paso Energy -------------------
Lab Code: ______ Case No.: SAS No.:
ltrix (soil/water ):_w_a_t_e_r ___ _ Lab Sample ID: --------98002988
Level (low/med): Date Received: 05/01/98 -----'---I Solids:
I
)
Concentration Units (ug/L or mg/kg dry weight): ug/L -----''----
I
I
I
I
I
I
I
I
' ' :CAs No.
' ' ' :7429-90-5
!7440-36-0
17440-38-2
h440-39-3
!7440-41-1
' :7440-43-9 ' 17440-70-2
:7440-47-3
\7440..:.49_4
/7440-50-8
:7439-89-6
17439-92-1 ' 17439-95-4 ' 17439-96-5
/7439-97-6
:7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
:7440-28-0 ' :7440-62-2
/7440-66-6
' ' '
' \Analyte
I ' A um.inum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
lcopper
!Iron
!Lead
/Magnesium
!Manganese
:Mercury
!Nickel
!Potassium
!selenium
!Silver
/Sodium
1Thallium
Vanadium
Zinc
.cyanide ------
lolor Before: ____ _
I
pl
Concentration
1850
2.5
1.0
48.6
0.1
0 .1
68.2
14.4
15.7
4. 6
' 2170 ' l 3. 8
' 910
' 83.9
' 0.20 ' 12. 4
1090
0.9
0.2
l 3990
0.8
3. 9
19. 3
Clarity Before:
Clarity After:
FORM I -IN
C Q
N
. ' B ' ' ' ' ' u '
B ' B ' u ' B ' ' '
B
B
' ' N• ' B ' ;
' u ' ' ' B
B
B N
B
B l I
u ; N ;
B ; ;
B ' ,_
' '
Texture:
Artifacts:
00029R
EPA SAMPLE NO.
M
W-11s
SDG No.: 863/864(icp)
838 (Hg)
p :---J""
p ' ' p ' p
p
p
p ' p
p
p :-
p ' ' p r ,.
p
p
p r.:... p
p ' ' p :-:r
p
PJ
p ,_
p
p
I
I
l Name:
U.S. E:?A -CLP
l
INORGA...~:c ANALYSIS DATA SEE~T
00030R
W-6s Dupe
[
. Code: Case No.: --------SAS No.: SDG No., 863/86-l(~c;,J
838 ( :l<;)
. =.i.x ( soil/water ) :
Ivel ( low/::Led):
\ Solids:
I
water ------Lab Sample ID: 98002990 ----..:..c...:...:. __
Date Received: 05/01/98 --------
j
I Ccncentration Units (ug/L or mg/kg dry weight): ug/L ------='----
' ' \A.nalvt.e ' -' '
Concent=ation C Q ' ' Ml ' ' ' I :7429-90-5 :Alm:iwn
\7440-36-0 !Anti..."nony
:7440-38-2 !Arsenic
!7440-39-3 \Barium
17440-41-7 !Beryllium
17440-43-9 :cadmium
:7440-70-2 !calcium
!7440-47-3 !chromium
!7440-48-4 !cobalt
17440-50-8 /copper
:7439-89-6 \Iron
h439-92-l lLead
17439-95-4 \Magnesium
!7439-96-5 p-ianga:iese
\7439-97-6 lMe:-cu=-y
/7440-02-0 \Nickel
!7440-09-7 l?otassium
17782-49-2 [selenium·
!7440-22-4 !silver
/7440-23-5 /sodium
17440-28-0 \Thalliu.."n;-'
/7440-62-2 /Vanadiu.~
!7440-66-6 !zinc
5620
l.5 B
N p :-T 7""----'--.,,--;----'----...;....p,;....:
I
I
I
I
I
I
8
' ' : /cyanide ,_ ____ ..;
Cclo.:-Eefo;:-e: ----
Dolor A!:t.e=:
Ccrnr.i.ent.s:
I
l.O
64. 0
t/.1! 5 -:.-0---zt}A'
0.1
2s 1. 0
24.8
76.2
ll. 0
5440
3. 6
731
184
0.20
18.5
1060
' 3. 0
' ' 0.4
/ 31900
:·.:• y:C -_Y.O I/,
1 • l. l
46. 4
clarity 3efore:
cla.=.:. ty .rt.£t.er:
B
B ! .a-· ; I l -' u :
a
B
! N*
a
! u
B
B
a N
' a ' !
! 3 !.• N
' a
:-
Texture:
p :--
p
p
P,
p ' ,-
p
p
p ,_
' p
p :J·
p ;
Pl
p
p ' ' p ' p '
p ' p
------
I
I
I
U.S. E::?.>. -CLP
1
INORGANIC .WALYSIS DATA Sc~~T
La::l Name: Cont:.=act: El Paso ~~ers-y -------------------lab Coc!e: Case No.: --------SdS No.:
Mat.=ix ( soil/water ) : water Lab Sample ID: 98002989 --------------
level (low/med): Date Received: 05/01/98 --------
~ Solids: ' I I
I Concentration Units (ug/L or mg/kg c!ry weight): ug/L
' ' ' ' I lCAS No. JAnalyte Concent=ation C
' ' ' ' ' :7429-90-5 iA unu.num 5870
Q
N
\i440-36-0 ' . -0.8 B :AntJ.Inony
I !7440-38-2 ' . 1.0 u :Arsenic
!7440-39-3 !Barium 62.9 B •
17440-41-7 iBeryllium 1,1. /';-.: -9---r cY" • )Y ~/ •
'
!
;
I i H40-4 3-9 :cadmium 0 .1 u
' ' :7440-70-2 :calcium 291.3 B
' ' 17440-47-3 I Chromium 3 7 .1
;
!7440-48-4 ' :cobalt. 80.4
!7440-50-8 ' 10. 5 3 I :cop9er
/7439-89-6 /I=on 5160
:7439-92-1 \Lead ! 4.0 ' l
/7439-95-4 /Magnesium ! 664 ' B
' I [7439-96-5 \Manganese ! 173 '
' /7439-97-6 :Mercury 0.20 u
' !Nickel /7440-02-0 25.9 B
'
)7440-09-7 ' 975. 6 :Potassium B
I !7782-49-2 !selenium 3. 8 B
)7440-22-4 )silver 0. 4 3
N
!7440-23-5 !Sodium : 31500 ! '
I /7440-28-0 !Thallium ; U, I -0 .Yt:14• 3 1:
' ' :7440-62-2 :vanadiu...'1\ 10. 6 6
' ' [7440-66-6 :zinc 50.9
N
' ' . ' :cyanide ' I
Color Be::ore:
Ilea lo= Af. ~e=:
cla.=ity Before:
Cla=ity A:!:'t.er: A.rti!acts:
00031R
W-6s
SDG No.: 863/864(ic?)
838 I Eg)
' ' M ' ' ' ' ' p ~-J
p ' ' pi-
p !
p ; ,// p :
p ' ,-
p
p
p :-
?
p ' _:
p
p
p :.rz
p
? ' ' p ~-,--' _, p
? ' p -p
p
------
gcomments:
FORM. I -IN
I
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
00032R
EPA SAMPLE NO.
W-12s
~ab
lab
Name: ECKENFELDER INC. Contract: El Paso Energy =====:..:....:==------------..:.:.::...:.......:::..:==-L-------__j
Code: Case No.: SAS No.: ------------------
latrix ( soil/water ) : ..:w:..:a:.t:.e:.r::... __ _ Lab Sample ID : __ ..;.9..:8..:0..:0.::2:..:9.::9.::lc__
Level (low/med): Date Received: 05/01/98 ___ _;__;._;._.;_ __
I Solids: /
I
I
I
concentration Units (ug/L or mg/kg dry weight): ug/L ----'-----
I
I
I
I
I
I
I
' ' ' CAS No. JAnalyte
' ' 7429-90-5 Aluminum
7440-36-0 Antimony
,7440-38-2 Arsenic
!7440-39-3 Barium
0 7440-41-7 !Beryllium
7440-43-9 ' Cadmium
7440-70-2 Calcium
7440-47-3 Chromium
17440-48-4 Cobalt
' 17440-50-8 Copper
' :7439-89-6 :Iron
!7439-92-1 !Lead
17439-95-4 \Magnesium
' ' /7439-96-5 /Manganese
7439-97-6 'Mercury
7440-02-0 Nickel
,7440-09-7 Potassium
17782-49-2 Selenium
/7440-22-4 silver ' \7440-23-5 ,Sodium
!7440-28-0 !Thallium
!7440-62-2 !vanadium
!7440-66-6 !zinc
/ /cyanide ,_ ____ _;
' ' ' concentration ' C Q ' ' ' !
' !
l ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' 2370
35.7
Clarity Before: Texture:
SDG No.: 863/864
: ' Mi
' '
' ' ' ' ' ' ' ' p
' ' p ' '
'
' ' ' ' ~
'
Color Before: ------
Color After: Clarity After: Artifacts: ----
-Comments:
FORM I -IN·
Name:
U.S. EPA -CLP
l
INORGANIC ANALYSIS DATA SHEET
00033R
EPA SAMPLE NO.
W-12i
I
I
[ ECKENFELDER INC. Contract: El Paso Energy --.:....:..=-;.:_=:..__________ ---....:....::.:==-'--------__;
Code: Case No.: SAS No.: SDG No.: 863/864 -----------------
latrix ( soil/water ) : ..:w:::a=.t.:.=e.::r __ _ Lab Sample ID: ---------98002992
Level (low/med): Date Received: 05/01/98 ___ ..;.__; ___ _
I Solids: I
I
I
Concentration Units (ug/L or mg/kg dry weight): ug/L ----=------
I
I
I
I
I
I
I
I
lfolor
-olor
CAS No. Analyte
: 7 429-90-5 Aluminum
\7440-36-0 Antimony
/7440-38-2 Arsenic
!7440-39-3 Barium
!7440-41-7 Beryllium
7440-43-9 Cadmium
7440-70-2 Calcium
7440-47-3 Chromium
' 17440-48-4 Cobalt
' 17440-50-8 Copper
' 17439-89-6 Iron
' 17439-92-1 Lead
' 17439-95-4 Magnesium
' 17439-%-5 Man anese g
17439-97-6 Mercury
h440-02-0 Nickel
' 17 440-09-7 Potassium
h7 82-4 9-2 Selenium
h440-22-4 Silver ' \7440-23-5 Sodium
\7440-28-0 Thallium
!7440-62-2 !vanadium
:7440-66-6 !zinc
~! _____ ~!cyanide
Before: -----
After:
lornrnents:
Concentration
' ' ' '
I ' ' ' 41.4 ' ' '
5.6
Clarity Before:
clarity After:
FORM I -IN
C
' ' ' ' ' ' ' ' ' ' ' B ' ' '
B
: ' Q Mi
' ' ' ' !
' '
' ' ' ' ' ' ' ' ' ' ' '
I I I ' ' ' ' ' ' ' ' p ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' p ' ' '
Texture: ------
Artifacts: ------
I
I
U.S. EPA -CLP
l
INORGANIC ANALYSIS DATA SHEET
Lab Name:
'1, Code:
ECKENFELDER INC. Contract: El Paso Energy --------"------------
[
trix (soil/water):
vel (low/med):
I Solids:
Case No.: SAS No.: ------------------
water Lab Sample ID: 98002993 ------'---
Date Received: 05/01/98 ---------------
I I Concentration Units (ug/L or mg/kg dry weight): ____ u~g~/~L:...._ __ _
I CAS No. Analyte Concentration C Q
I 7429-90-5 Alwninum
7440-36-0 Antimony
7440-38-2 Arsenic
7440-39-3 Barium
I 7440-41-7 Beryllium ' ' ' ' '
7440-43-9 Cadmium ' ' ' '
!7440-70-2 Calcium ' ' ' '
I 17440-47-3 Chromium ' ' ' ' ' '
7440-48-4 Cobalt ' ' ' '
7440-50-8 Copper ' ' ' '
I ' 17439-92-1 Lead
' 17439-95-4 Magnesium
'
, 7439-89-6 Iron 1120 ' ' ' '
' ' ' '
'7439-96-5 Manganese 33.2 ' ' ' '
I 7 439-97-6 Mercury
7440-02-0 Nickel
:7440-09-7 Potassium
I i
I
!7782-49-2 Selenium
17440-22-4 Silver ' .
/7440-23-5 Sodium
'
!7440-28-0 Thallium ' ' ' '
I ! 7 440-62-2 :vanadium
:7440-66-6 !zinc
' /cyanide ' '
I
Color Before: Clarity Before: Te.xture:
o·oo34R
EPA SAMPLE NO.
W-18s
SDG No.: 863/864
I ' ' Mi ' ' '
j
!
; ' ' '
p
p
' ' ' '
lolor -------
After:
'omments:
I
I
Clarity Af cer: Artifacts: ------
FORM I -IN
U.S. EPA -CLP
l
I
I INORGANIC ANALYSIS DATA SHEET
llf'ab Name:
l,ab Code:
ECKENFELDER INC.
Case No.:
Contract:
SAS No.: -------
ratrix (soil/water ):_w_a_t_e_r;__ __
Level (low/med): I Solids:
Lab
Date
Sample ID:
Received:
I
00035R
EPA SAMPLE NO.
W-30i
El Paso Energy
SDG No.: 863/864
98002994
05/01/98
{(t{ / 4~ I y1-1t, I
I
I
Concentration Units (ug/L or mg/kg dry weight): ug/L ----=------
I
I
I
I
I
I
I
' ' ' :cAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
:7440-41-7 ' . •7440-43-9 : .
:7440-70-2
i7440-47-3
:7440-48-4
:7440-50-8
:7439-89-6
' '7439-92-1
7439-95-4
7439-96-5
,7439-97-6 ' :7440-02-0 ' :7440-09-7
:7782-49-2
7440-22-4
7440-23-5
7440-28-0
: 7 440-62-2
!7440-66-6
' ' '
'Color Before:
Color After:
ICornrnents:
I
Analyte
Aluminum
Antimony
Arsenic
:Barium
' :Beryllium
!cadmium
!calcium
!chromium
!cobalt
' 'Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
!sodium
!Thallium
:vanadium
!zinc
!cyanide
' ' ' ' ' ' ' ' ' Concentration C Q M ' ' ' ' ' ' ' ' !
' ' !
'
' ' ' '
1590 p
23.0
11
Clarity Before: Texture: ------
Clarity After: Artifacts: ------
FORM I -IN
I
I
Ir ab Name:
ab Code:
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
ECKENFELDER INC. Contract: El Paso Energy ..::.c..c..:......:..:::==.:.-=-'-----------
Case No.: SAS No.: -----------------
l?trix ( soil/water ) : _w_a_t_e_r __ _ Lab Sample ID: ---------98002996
Level (low/med): Date Received: 05/01/98 ___ ..;._..;:;.;--'-:.....--
I Solids:
I j
Concentration Units (ug/L or mg/kg dry weight): ug/L ----"------
I ' ' ' ' ' ' ' ' ' CAS No. Analyte ' Concentration C Q ' ' ' ' ' I 7429-90-5 Aluminum ' 7440-36-0 Antimony :
7440-38-2 Arsenic
7440-39-3 Barium ' '
00036R
EPA SAMPLE NO.
W-22s
SDG No.: 863/864
: ' M ' ' ' ' '
I
I
I
I
7440-41-7 Beryllium ' i
- -
7440 43 9 Cadmium
I
I
I
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
,7439-96-5 ' 17439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
:7440-23-5
!7440-28-0
J1440-62-2
:7440-66-6
' ' '
aolor Before:
~olor After:
lomments:
I
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
cyanide
' ' ' ' '
1820 p
' ' ' !
' ' ' ' ' 523 p ' ' ' ' !
' '
' ' ' ' ' '
Clarity Before: Texture: -----
Clarity After: Artifacts: -----
FORM I -IN
I
I
[
Name:
Code:
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SEEET
ECKENFELDER INC. Contract: El Paso Energy ------~-------------
Case No.: SAS No.: --------
Lab Sample ID: 98002995 rtrix ( soil/water ) : _w_a_t_e_r __ _ ---------
Level (low/med): Date Received: 05/01/98
I Solids:
I I
I
Concentration Units (ug/L or mg/kg dry weight): ug/L ---~~----
I
I
I
I
I
I
I
I
' ' ' CAS No. !Analyte
' !
17429-90-5 •Aluminum
!7440-36-0 Antimony
:7440-38-2 Arsenic
!7440-39-3 Barium
!7440-41-7 Beryllium
17440-43-9 Cadmium
' :7440-70-2 Calcium
' 17440-47-3 Chromium
17440-48-4 Cobalt
' 7440-50-8 Copper
7439-89-6 Iron
7439-92-1 Lead
7 439-95-4 Magnesium
17439-96-5 Manganese
7439-97-6 Mercury
7440-02-0 Nickel
,7440-09-7
17782-49-2
17440-22-4 ' ·:7440-23-5
!7440-28-0
!7440-62-2
!7440-66-6
' ' ' r-------,
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
cyanide
901or Before:
'tolor After:
Concentration
' ' ' '
36.1
' '
2.2
'
i
' ' ' ' ' '
Clarity Before:
clarity After:
C
B
B
' '
' ' ' Q ' '
' ' ;
' ' ' '
' ' '
' '
Texture:
Artifacts:
00037R
EPA SAMPLE NO.
W-l0i
SDG No.: 863/864
M
p
' . !
' ' p
----------
lomments:
I
I FORM I -IN
I
I
Lab Name:
Im· Code:
U.S. EPA -CLP
1
00037AR
E?A SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
W-20i
ECKENFELDER INC. Contract: El Paso Energy
.;:;___::.:..::.:::=='--==:.:..:-----------
Case No.: --------SAS No.:---------SDG No.: 863/86-!
11atrix ( soil/water ) :
level (low/med):
water Lab Sample ID: 98002997 ---------
Date Received: 05/01/98 ---------------
I solids:
I I Concentration Units (ug/L or mg/kg dry weight): ug/L ----"---'---
I
I
I
I
I
I
I
I
I
Color
lcolor
' ' ' CAS No. lAnalyte
:7429-90-5 Aluminum
/7440-36-0 Antimony
!7440-38-2 Arsenic
' · :7440-39-3 Barium
/7440-41-7 Beryllium
!7440-43-9 Cadmium
l7440-70-2 Calcium ' ' /7440-47'-3 Chromium
' :7440-48-4 Cobalt
' 17440-50-8 Copper
!7439-89-6 Iron
' :7439-92-1 Lead
' :7439-95-4 Magnesium
:1439-96-5 Manganese
\7439-97-6 Mercury
/7440-02-0_ Nickel
l7440-09-7 Potassium
l7782-49-2 Selenium
[744.0-22-4 Silver
!7440-23-5 Sodium
\7440-28-0 Thallium
/7440-62-2 Vanadium
]7440-66-6 Zinc
' _: _____ ~cyanide
Before: -----
After:
.Comments:·
I
' ' ' Concentration ' C Q M ' ,
' ' :
' '
: : : : ' '
18 .1 B p
1.6 ' B ' p ' '
' '
' :
' '
' ! : :
'
clarity Before: Texture: ------
Clarity After: Artifacts: ------
FORM I -IN
I
I
Lab Name:
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
00038R
EPA SAMPLE NO.
W-20s
L
ECKENFELDER INC. Contract: El Paso Energy _.c.c:..c...c..:..::::..::.:.c...c=..::..c..._________ ------..:..e.....L _______ __.
Code: Case No. : _______ _ SAS No.: ________ _
latrix ( soil/water ) : .cw:.:a:..t:..e:..r __ _
Level ( low/med) :
Lab Sample ID: 98002998 _____ ;_;_ __ _
Date Received: 05/01/98 _ ___;=..:.=..:...:.. __
I Solids:
/ I
I
I
Concentration Units (ug/L or mg/kg dry weight): ___ :.:u:..g~/'-'L~---
I
I
I
I
I
I
I
' ' ' CAS No. !Analyte
' ' ,7429-90-5 Aluminum
7440-36-0 Antimony
7440-38-2 Arsenic
7440-39-3 Barium
7440-41-7 Beryllium
7440-43-9 Cadmium
7440-70-2 Calcium
7440-47-3 Chromium
7440-48-4 :cobalt
' ' !7440-50-8 :copper
:7439-89-6 :Iron
' ' :7439-92-1 !Lead
!7439-95-4 /Magnesium
\7439-96-5 !Manganese
:7439-97-6 /Mercury
!7440-02-0 JNickel
1 7440-09-7 1Potassi:wn
7 7 82-49-2 Selenium
7440-22-4 Silver
,7440-23-5 Sodium
! 7 440-28-0 Thallium
/7440-62-2 :vanadium
\7440-66-6 !zinc
,! _____ \cyanide
l(olor Before:
.olor After:
Concentration C Q
' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' '
' ' ' ' ' '
12 3 u
' ' ' ' ' '
' ' ' ' 0.4 ' B ' r
' '
' ' i
' ' ' '
Clarity Before: Texture:
Clarity After: Artifacts:
SDG No.: 863/864
' M
' ' ' ' ' '
p
'
p
'
' '
----------
lomments:
I FORM I -IN
I
I
Lab Name:
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
ECKENFELDER. INC. Contract: El Paso Energy -------'---------------
00039R
EPA SAMPLE NO.
FB42998
lab Code: Case No.: --------SAS No.:---------SDG No.: 863/864
ratrix (soil/water) :_w_a_t_e_r __ _
Level (low/med):
Lab Sample ID: ---------98002999
Date Received: ---------05/01/98
I Solids: I I
I
I
Concentration Units (ug/L or mg/kg dry weight): ug/L ----~----
CAS No. Analyte concentration
7429-90-5 Aluminum
7440-36-0 Antimony
7440-38-2 Arsenic
17440-39-3 Barium
: 7 440-41-7 Beryllium
17440-43-9 Cadmium
7440-70-2 Calcium
7440-47-3 Chromium
,7440-48-4 Cobalt
' 17440-50-8 Copper
' '7439-89-6 Iron ' 12.3 ' 7439-92-1 Lead ' '
I
I
I
I
I
I
I
7439-95-4 M~gnesiurn !
7439-96-5 Manganese
17439-97-6 Mercury ' : 7 440-02-0 Nickel
!7440-09-7 Potassium
:7782-49-2 Selenium
:7440-22-4 Silver
' ' --,7440 23 5 ,sodium
17440-28-0 Thallium
!7440-62-2 Vanadium
:7440-66-6 Zinc
' : :cyanide _____ _,
_.=olor Before:
11:olor After: -----
fomments:
I
' -~Ii, I '
Clarity Before:
Clarity After:
FORM I -IN
'
' ' '
C
u
.,B"' (/
_,
'
Q
' ' ' ' ' ' ' ' ' '
Texture:
Artifacts:
M
p
p
I
U.S. EPA. -CLP
1
00040R
EPA. SAMPLE NO. I INORGANIC ANALYSIS DA.TA SHEET
I Name: ECKENFELDER INC.
Case No.: I Code:
rix ( soil/water ) : water
l el (low/med):
olids:
I
------
I W-5s
Contract:_E_l_P_a_s_o __ E_n_e_r~g~y'--'-------------~
SAS No.:
Lab Sample ID: 98003001 --------
Date Received: 05/0l/98
j
SDG No.: 863/864(icp)
838 (Hg)
I Concentration Units (ug/L or mg/kg dry weight): ug/L ---~'----
I
I
I
I
I
I
I
'olor
tlor
;
' :CAs No.
' ' ' 7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
,7440-43-9
' 17440-70-2
' '7440-4 7-3
7440-48-4
7440-50-8
7439-89-6
17439-92-1
17439-95-4
17439-96-5
' :7439-97-6
/7440-02-0
' 17440-09-7
/7782-49-2
!7440-22-4
17440-23-5
7440-28-0
7440-62-2
7440-66-6
' ' '
;
' JAnalyte
' ' :Al.um.J.num·
!Antimony
!Arsenic
/Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
' Lead
!Magnesium
/Manganese
Mercury
Nickel
Potassium
•Selenium
Silver
Sodium
Thallium
' I Vanadium
!zinc ' . :cyanide -----~
Before: ----
After:
Comments:
' ' Concentration
2510
1.3
1.0
' 265
0.3
0.1 ' 402
a.a
58.2
9. 5
2930
6.9
1920
1120
10.6
18.3
' 3220 ' 2.5
0.2
19100
a. a
' 4.0
' 59.6 '
Clarity Before:
Clarity After:
FORM I -IN
C Q M
' ' N ' p
' ' '
' B ' ' p
' ' ' u ' p, ' ' P!
.B Pj
u Pl
B p ' ' ' ' B p ' ' ' '
' ' p
' ' ' B I p
' p
N* p T
B '
p
! p
' p ' ' B p ' ' '
' B ' p
' ' ' 8 ' N p
' ' ' u ' p
' '
' p
u N p ,__
B Pi
' p ' ' '
Texture:
Artifacts: ------
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET.
00041R
EPA SAMPLE NO.
W-24s
I
I 1: Name: ECKENFELDER INC. Contract: El Paso Energy -----------------------'-''-'-"-'----------'
Code:
ratrix (soil/water
Level (low/med): I Solids:
Case No.:
) : water
SAS No.: -------
Lab Sample ID:
Date Received:
I Concentration Units (ug/L or mg/kg dry weight):
I ' ' ' ' ' ' ' ' :cAS No. Analyte ' Concentration C ' ' ' ' ' ! ' I :7429-90-5 •Aluminum
7440-36-0 Antimony
7440-38-2 Arsenic
I 7440-39-3 Barium
17440-41-7 Beryllium ' ' :7440-43-9 Cadmium ' ' !7440-70-2 Calcium
I i I ' 17 440-4 7-3 Chromium
' 17440-48-4 Cobalt
' 17440-50-8 Copper ' ' ' ' ' ' 17439-89-6 Iron ' 65700 I ' ' ' 17439-92-1 Lead ' ' ' ' ' ' 7439-95-4 :Magnesium
7439-.96-5 1Manganese 2590
I 7439-97-6 Mercury
,7440-02-0 Nickel ' 7440-09-7 Potassium
I 7782-49-2 Selenium ' 7440-22-4 Silver·
7440-23-5 Sodium
7440-28-0 Thallium ' : I ,7440-62-2 1Vanadium -
17440-66-6 ' . :z.1.nc
' ' . ' :cyanide '
I
lcolor •Before: Clarity Before:
Color After: clarity After:
.comments:
I FORM I -IN
SDG No.: 863/864
98003002 ---------
05/01/98
J
ug/L
' ' Q M
'
' ' ' ' ' '
I i I ' ' ' ' ' ' ' ' ' p ' ' ' • ' ' ' ' p
' '
i
' ' ' '
Texture:
Artifacts:
U.S. EPA -CLP
1
I
I
1:
INORGANIC ANALYSIS DATA SHEET
Name: ECKENFELDER INC. Contract:
Code: Case No.: SAS No.:
latrix ( soil/water ) : _w_a_t_e_r __ _
Level (low/med):
Lab Sample ID:
Date Received:
I solids:
00042R
EPA SAMPLE NO.
W-20s Dupe
El Paso Energy
SDG No.: 863/864
98003003 ---------
05/01/98
I
I
I
Concentration Units (ug/L or mg/kg dry weight): ug/L ----"'------
I
I
I
I
I
I
I
I ' ' ' ' :cAs No. lAnalyte ' ' ' ' ' 7429-90-5 :Aluminum
7440-36-0 !Antimony
7440-38-2 !Arsenic
7440-39-3 !Barium
7440-41-7 1Beryllium
7440-43-9 Cadmium
,7440-70-2 Calcium
'7440-47-3 Chromium
7440-48-4 Cobalt
7440-50-8 Copper
, 7439-89-6 :Iron ' ' '7439-92-1 :Lead
7439-95-4 Magnesium
7439-96-5 Manganese
,7439-97-6 Mercury
17440-02-0 Nickel ' !7440-09-7 Potassium
!7782-49-2 Selenium
!7440-22-4 Silver
!7 440-23-5 Sodium
:7440-28-0 Thallium
!7440-62-2 Vanadium
!7440-66-6 Zinc
' t Cyanide ,_ ____ ...;
llolor Before:
lolor After:
lornrnents:
I
Concentration C Q M
:
i
I ' ' ' ' ' ' ' ' ' ; ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' 357 p
' ' ! ' ' ' ' 7. 6 B p !
! ' I
I ' I ; ; '
' . ' ' ' ' '
Clarity Before: Texture: ------
Clarity After: Artifacts: ------
FORM I -IN
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
I
Lab Name: ECKENFELDER INC. Contract: El Paso Energy
~ Code: Case No.: SAS No.:
ltrix (soil/water
vel ( low/med) :
I solids:
) : water
---------------
Lab Sample ID: 98003004 -------'---
Date Received: 05/01/98 ---------
Concentration Units (ug/L or mg/kg dry weight): ____ u_g:.;../L ___ _
CAS No. Analyte Concentration C Q
7429-90-5 Aluminum
Antimony !
00043R
EPA SAMPLE NO.
EB42998
SDG No.: 863/864
M
I
I
I
I
I
I
I
I
I
'I
, 7440-36-0
!7440-38-2 T
Color
Iler
Arsenic
7440-39-3 Barium
7440-41-7 Beryllium
7440-43-9 Cadmium
7440-70-2 Calcium
,7440-47-3 Chromium
' J7440-48-4 Cobalt
' :7440-50-8 '
Copper
17439-89-6 Iron
:7439-92-1 Lead
17439-95-4 Magnesium
h439-96-S Manganese
!7439-97-6 Mercury ' :7440-02-0 Nickel ' :7440-09-7 Potassium : -:7782-49-2 Selenium
!7440-22-4 Silver
!7440-23-5 Sodium
l7440-28-0 1Thallium
\7440-62-2 Vanadium
!7440-66-6 Zinc
' : cyanide '------'
Before: ----
After:
rmments:
I
I
12.3
0.3
' C '
'
!
' ' ' '
Clarity Before:
clarity After:
FORM I -IN
u
' ' B
' ' ' ' ' '
' ' ' ' ' '
p
' ' ' ' p ' ' .
' ' ' ' _,
' ' ' ' '
Texture: ------
Artifacts: -----
U.S. EPA -CLP
1
00043AR
I INORGANIC ANALYSIS DATA SHEET
Name: ECKENFSLDER INC. Contract: El Paso Energy ..::.:=c..::..:==-=:..::..:.---------
Code: Case No.: SAS No.: -----------------
,fatrix ( soil/water ) : _w_a_t_e_r __ _
Level (low/med):
Lab Sample ID: 98003005 ---------
Date Received: 05/01/98
' I
Solids:
___ _;_....c.c..::...:.... __
Concentration Units (ug/L or mg/kg dry weight): ug/L ----"-----
: ' :CAs No. Analyte ' ' ' :7429-90-5 Aluminum
!7440-36-0 Antimony
:7440-38-2 Arsenic
!7440-39:_3 Barium
' :7440-41-7 :Beryllium
!7440-43-9 !cadmium
!7440-70-2 lcalciurn
!7440-47-3 Chromium
' 17440-48-4 Cobalt
Concentration C Q
' '
!
' '
1260
46.4
'
EPA SAMPLE NO.
W-22i
SDG No.: 863/864
' ' M ' ' '
p
p
I
I
I
I
!7440-50-8 Copper
!7439-89-6 Iron
:7439-92-1 Lead
/7439-95-4 Magnesium ! 1439-9 6-5 :Manganese
7439-97-6 !Mercury
7440-02-0 :Nickel
7440-09-7 !Potassium
7782-49-2 Selenium
7440-22-4 Silver
' '
lea: ,r
olor
7 440-23-5 Sodium
7440-28-0 :Thallium
7440-62-2 !vanadium
:7440-66-6 !zinc
! !cyanide ,_ ____ ....;
Before: ----
After:
lomments:
I
' '
'
: : ' : ' ' ' ' ' -
Clarity Be:"ore: Texture: ------
Clarity Aft·er: Artifacts: -----
FORM ,. -IN
'I
'
I
U.S. EPA -CLP
l
INORGANIC ANALYSIS DATA SHEET
Lab Name: ECKENFELDER INC. Contract: El Paso Energy
Code: Case No.: _______ _ SAS No.: ---------
,1·
1
trix ( soil/water ) :
vel ( low/med) :
water
------
Lab Sample ID :. ___ 9_8_0_0_3_0_0_:6 __
Date Received: 05/01/98 /--
Concentration Units (ug/L or mg/kg dry weight) : ____ u_g=.;../_L __ _
11
t
I
:f
i
1:
CAS No. Analyte
7429-90-5 Aluminum
7440-36-0 Antimony
7440-38-2 Arsenic
7440-39-3 Barium
7440-41-7 Beryllium
7440-43-9 CadmiUlll
7440-70-2 Calcium
7440-47-3 Chromium
7440-48-4 Cobalt
7440-50-8 Copper
7439-89-6 Iron
7439-92-1 Lead
7439-95-4 Magnesium
7439-96-5 Manganese
7439-97-6 Mercury
7440-02-0 Nickel
7440-09-7 Potassium
7782-49-2 Selenium
7440-22-4 Silver
7440-23-5 Sodium
7440-28-0 Thallium
! ! !
Concentration ' C Q
' '
' ' ' ' ' '
' ' ' ' ' '
I i i i
'· 12. 3 ' u ' ' ' ' ' '
' ' ' ' 27.4 ' '
'
' '
'
' ' ' ' ' ' ' ' ' ' ' '
00044R
EPA SAMPLE NO.
M
p
p
W-29i
SDG No.: 863/864
'
' ' ' ' ' '
i
' ' ' .,
' '
'
,t ,, 7440-62-2 Vanadium ' ' -' ' ' ' !
7440-66-6 Zinc
1Cyanide
,I
Color llor Before: ----
After:
Clarity Before:
Clarity Afte:r:
Tex':.ure: ------
Artifacts: -----
lmments:
I FORM I -IN
U.S. EPA -CLP
l
00045R
EPA SAMPLE NO. I
I INORGANIC ANALYSIS DATA SEEET
Name: ECKENFELDER INC.
Code:
[t'trix ( scil/water ) :
fevel (low/med):
Case No.:
water
Contract:
SAS No.: --------
El Paso Energy I W-9s
---------SDG No.: 865/866(icp)
838 (Hg)
Lab Sample ID: 98003118 ---------
Date Received: 05/07/98 ------t1solids:
Concentration Units (ug/L or mg/kg dry weight): ug/L ____ ::,_ ___ _
,,,
i ,,
j,
' ' ' ' ' ' :cAS ' No. iAnalyte
' ' ! !
:7 429-90-5 !Aluminum ' . ' :7440-36-0 Antimony
i7440-38-2 Arsenic
\7440-39-3 Barium
!7440-41-7 Beryllium
7440-43-9 :cadmium
7440-70-2 :calcium
7440-47-3 Chromium
--,7440 48 4. Cobalt
' :7440-50-8 Copper
:7439-89-6 Iron
:7439-92-1 1Lead
' :7439-95-4 Magnesium
/7439-96-5 Manganese
i7439-97-6 Mercury
:?440-02-0 Nickel
h440-09-7 Potassium
' :7782-49-2 Selenium
h 440-22-4 Silver ' !7440-23-5 Sodium
:7440-28-0 Thallium
\7440-62-2 Vanadium
!7440-66-6 Zinc
' 1 Cyanide i-------,
'
~;°lor Before:
lolor Afte=:
'omments:
I
Concentration
769
1.0
::J.-:-0' ;, c;
27. 7
0. l
0.l
64.3
10.2
2.1
l. 7
1080
l. 3
• 1100
• 36.5 . 0.20
8.8
1120
0.6
0.2 -35a0
0.8
1.7
74.3
Clarity Before:
Clarity After:
FORM I -IN
C Q M
E p
B p
_,Z'•i ,. p
' B ' p
' ' ' B ' p ' ' ' B ' p
' '
' B ' p ' ' ' ' ' p ' ' ' B ' ' p '
B p
p
B p
B ' ' p ' !
' ' p ' ' '
' u ' i CV
: a : p '
B ' p !
u : N p !
u ' ' p ' ' ' ' B . p
u p
B + p
p
Texture: -----
Artifacts:
U.S. E?A -CLP
l
00046R
E?A SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
W-9s Dupe
Name: ECKENFELDER INC. Contract: El Paso Energy
Code: Case No.: --------SAS No.: SDG No.: 865/866(ic;:,) ---------838 (Hg)
ltrix (soil/water
' vel ( low/med) :
) : water Lab Sample ID: ---------
Date Received:
98003119
05/07/98
l'Solids:
Concentration Units (ug/L or mg/kg dry weight): ug/L ----'-----
I
I
I
I' ,.,
I
t
I
I
'11
,_,Coler
,lolor
' ' ' :CAs No. Analyte
' ' :
:7429-90-5 Aluminum
!7440-36-0 Antimony
:7440-38-2 Arsenic
:7440-39-3 Barium
\7440-41-7 Beryllium
!7440-43-9 Cadmium
!7440-70-2 Calcium
!7440-47-3 Chromium
' \7440-48-4 Cobalt
!7440-50-8 Copper
:7439-89-6 Iron
!7439-92-1 Lead
!7439-95-4 Magnesium
' /7439-96-5 Manganese
!7439-97-6 Mercury
Ii 440-02-0 Nickel
h 440-09-7 Potassium
' /7782-49-2 Selenium
:7440-22-4 Silver
/7 440-23-5 Sodium
/7440-28-0 Thallium
/7 440-62-2 Vanadium
!7440-66-6 Zinc : 1 cyanide ------'
Before:
After:
romments:
I
Concentration
1760
I 0.7
' -=-~ (,(.' ' ; 35.5 ' ' 0.l ' ' l.0 ' ' 65.6 ' ' ll.5 ' 2.6
3.4
2430
' l. 9 ' ' 1310 ' ' 52.9 ' ' 0.20 '
' 9. 5
' 1480
' 0.6
' 0.2
3470
0.8
3.7
Bl. 5
Clarity Before:
Clarity After:
FORM I -IN
' : ' I C Q M '
E p T
u : p
,!Y(/ ' : p
' B ' ' p
' ' ' B ' i p ' ' ' '
' u ' ' p ' ' ' '
' B p ' ' ' ' p ' ' '
B p
B p
p
' B p ' '
' B ' p ' ' ' ' p ' ' ' u ' :cv! ' B ' ' p '
B i P:
u N ' p i
u ' p ' ' ' B ' ' p ' ' ' ' u p
B ..!. p
p
Texture:
Artifacts:
U.S. EPA -CLP
l
00047R
EPA SAMPLE NO. I-
I INORGANIC ANALYSIS DATA SHEET
Lab Narne: ECKENFELDER INC.
LI Code:
l rix (soil/water
L el (low/med):
Case No.:
) : water
Purge Water
Contract: El Paso Energy
--------SAS No.: ________ SDG No.: 865/866(icp)
838 ( Bg)
Lab sample ID: __ ~9_8_o_o_3~1~2_0 __
Date Received: 05/07/98 ___ ..;_ ____ _
I I-Concentration Units (ug/L or mg/kg dry weight): ug/L ---~'-'------
,1:
I
:1 ,,.
I:
Color
,Jlor
' ' ' ' CAS No. 'Analyte
7429-90-5 Aluminum
7440-36-0 Antimony
7440-38-2 Arsenic
7440-39-3 Barium
7440-41-7 Beryllium
7440-43-9 Cadmium
7440-70-2 Calcium
7440-47-3 chromium
7440-48-4 Cobalt
7440-50-8 Copper
7439-89-6 Iron
7439-92-1 Lead
7439-95-4 Magnesium
7439-96-5 Manganese
7439-97-6 Mercury
7440-02-0 Nickel
7440-09-7 Potassium
7782-49-2 Selenium
:7440-22-4 Silver
!7440-23-5 Sodium
:7440-28-0 Thallium
!7440-62-2 Vanadium
!7440-66-6 Zinc
' : :cyanide ,_ ____ ...;
Before: -----
After:
rmments:
Concentration C Q M
1810 E ' p T
1.6 B p
1.8 B P!
19.4 B p ' ' ' 0.2 B p ' ' ' ' 0.1 ' B p
' 23000 p ' ' 22.9 p ' ' 0.6 B p ' ' 4.3 B p ' ' 754 ' p
' 1.1 B ' p ' ' ' 1170 B ' p ' . ' ' 16.l ' P, ' . ' 0.20 u ' CV!,
5.5 ' B p i
38200 ' p i
' 4.0 ' B N p;
; 0.5 ' B p
' ' ; 40200 ' p
' ' 0.8 ' u ' p ' ' 19.7 ' B ! ' p ' ' ' ' 11.5 ' B ' ' p ' ' ' ' ' ' ' ' ' ' ' ' '
Clarity Before: Texture: -----
Clarity After: Artifacts: -----
,J----------
I FORM I -IN
00048R U.S. EPA -CLP
1 EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Name: I W-28i
~E~C~KE=N~F~E~L=D:..::E~Rc....:I..:N..:C~-c_ __________ contract:....::E_l_P_a.:.s~o~E.::n:..::e=r2gy.,_L_ __________ ~
Code: Case No.: --------SAS No.: _________ SDG No.: 865/866(icp)
Matrix ( soil/water ) : __ w=a-=t-=e.::r __ 4el (low/med):
Lab Sample ID: __ .;;.9.:.8.:.0.:.0..:3.=l.=2.=l __
Date Received: 05/07/98 ___ ..;_.:..:.~---
'Solids: _ /
~, I, Concentration Units (ug/L or mg/kg dry weight): ____ u_g=-/L ___ _
:I
I'
I
I
i
/I
Iler
CAS No. Analyte
7429-90-5 Aluminum
!7440-36-0 Antimony
;7440-38-2 1 Arsenic
;7440-39-3 Barium
7440-41-7 Beryllium
7440-43-9 Cadmium
7440-70-2 .Calcium
7440-47-3 ·:chromium
:7440-48-4 ' Cobalt
' :7440-50-8 Copper
' :7439-89-6 Iron
7439-92-1 Lead
7439-95-4 Magnesium
7439-96-5 Manganese
7439-97-6 Me 1 rcury
7440-02-0 ;Nickel
!7440-09-7 !Potassium
i7782-49-2 'Selenium
i7440-22-4 Silver
J7440-23-5 Sodium
;7440-28-0 Thallium
i 7 440-62-2 1 Vanadium
/7440-66-6 !zinc
! !cyanide ;.... ____ _
Before:
Concentration C Q
' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' '
' 573 ' ' ' ' ' ' ' ' ' ' '
' ' ' ' ' ' '
8. 6 ' B ' ' ' : ' ' '
'
'
' i
! ' ' ' ' .
' ' ' ' ' ' ' ' ' ' '
Clarity Before: Texture:
M
p
p
'
---------,jlor After:
Comments:
t
I
I
Clarity After: Artifacts: -----
FORM I -IN
838 (Hg)
Name:
U.S. EPA -CLP
l
INORGANIC ANALYSIS DATA SHEET
00049R
EPA SAMPLE NO.
W-19s I
1 ECKENFELDER INC. Contract: El Paso Energy l
------------------------'"'-'---'--· _________ _J
Code: Case No.: --------SAS No.: SDG No.: 865/866(icp) ---------trix (soil/water) : __ w_a_t_e_r __
Level (low/med):
folids:
,,·
Lab Sample ID: 98003122 ---------
Date Received: 05/07/98 ---------
Concentration Units (ug/L or mg/kg dry weight): ug/L ----=------,,,
:a.
.t
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3 --7440 48 4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
17439-96-5
:?439-97-6 ' 17440-02-0 ' 17440-09-7
h1a2-49-2 ' !7440-22-4
!7440-23-5
J7440-28-0
/7440-62-2
!7440-66-6
' ' '
' ' ' !Analyte
' ' Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
,Cobalt
' :copper
liron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
1 Silver
!sodium
!Thallium
!vanadium
!zinc
!cyanide ~-----
'. ' ' ' ' Concentration C Q '
' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' '
1670
' ' ' ' ' ' : ' '
' 36.4 ' ' ' ' ' ' ! ! '
! ' ' !
; ' ! '
i ' ! :
; i ' ' ' ' ' ; ' ; ' ' ' ' '
Clarity Before: Texture:
I ' M
'
p
p
'
Iler Before:
' lor After:
-----
Clarity After: J..rtifacts:
rmrnents:
I
FORM I -IN
838 (Hg)
I
Lab Name:
LI Code:
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
00049AR
EPA SAMPLE NO.
I W-5i
ECKENFELDER INC. Contract: El Paso Energy
-----------------------C..<a.....!.. ________ _;
Case No.: --------SAS No., ________ SDG No.: 865/866(icp)
838 (Hg)
Matrix (soil/water): water lel (low/med): -~---
Lab Sample ID: 98003123 ---------
Date Received: 05/07/98 ---------
tolids:
·--·
Concentration Units (ug/L or mg/kg dry weight): ug/L ----'-----
-· 'I .,
t
I
I
I
' ' ' ICAS No. Analyte ' ' ' :7429-90-5 Aluminum
:7440-36-0 Antimony
:7440-38-2 Arsenic
7440-39-3 Barium
7440-41-7 Beryllium
7440-43-9 Cadmium
17440-70-2 Calcium
!7440-47-3 Chromium
!7440-48-4 Cobalt
!7440-50-8 Copper
' :7439-89-6 Iron
17439-92-1 Lead
' 17439-95-4 Magnesium
\7439-96-5 Manganese
!7439-97-6 Mercury
17440-02-0 Nickel
:7 440-09-7 Potassium
7782-49-2 Selenium
7440-22-4 Silver
17440-23-5
\ 7 440-2 8-0
/7440-62-2
!7440-66-6
'
Sodium
Thallium
Vanadium
Zinc
: Cyanide -------i
Color Before: -----liar After:
I
I
concentration C Q M
'
' '
' ' ' ' ' ' ' ' ' ' ' '
' ' ' '
' ' ' ' ' ' ' '
1020 p
' ' ' ' ' '
' ' ' '
46.7 ' p !
! !
' ' ! !
! ;
: :
; .
' ;
' ' ' ' '
Clarity Before: Texture: -----
Clarity After: A.1.-tifacts: -----
FORM I -IN
·I
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1'j' Name:
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
ECKENFELDER INC. Contract:
00049BR
EPA SAMPLE NO.
El Paso
W-16s
Energy I
LI, Code: Case No.: --------SAS No.: _________ SDG No.: 865/866(icp)
frix (soil/water ) , __ w_a_t_e_r __
Level (low/med):
•Jo lids:
Lab Sample ID, 98003124 ___ ...;:..:c=...:;_ __
Date Received: 05/07/98
I·
1· ,,,
Concentration Units (ug/L or mg/kg dry weight): ug/L ---~'-'------
t
I
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I
' ' ' lCAS No. Analyt:e
I ' ' ,7429-90-5 ' Aluminum
!7440-36-0 Antimony
/7440-38-2 Arsenic
!7 440-3 9-3 Barium
!7440-41-7 Beryllium
/7440-43-9 Cadmium
!7440-70-2 Calcium
! 7 440-4 7-3 Chromium
' 17440-48-4 Cobalt
' 17440-50-8 Copper
' 17439-89-6 Iron
/7439-92-1 Lead
I
!7439-95-4 Magnesium
:]439-96-5 Manganese
I 74 39-97-6 Mercury
h440-02-0 Nickel
17440-09-7 :Potassium
h1s2-49-2 1Selenium ' !7440-22-4 Silver
!7440-23-5 Sodium
!7440-28-0 :Thallium
!7440-62-2 !vanadium
i7440-66-6 !zinc
! !cyanide ,_ ____ ...,
Before: ----
After:
,,mments:
' ' ' ' Concentration ' ' ' '
' 999
: 0.7
1.0
44.2
0.2
0.1
133.6
11.3
2.6
2.1
721
1.1
1120
41 3
0.20
10.2
1330
0.8
0.2
10700
0.8
' 1.1
88.5
Clarity Before:
Clarity After:
FORM I -IN
I ' ' ' ' C ' Q M '
E p
u p
u p
B ' p
' ' B ' p
' ' B ' p ' B p
p
B p
B p
p
B p
B p
. ' p
' u ! ,CVi
B : p
B ' p
B : N p
u ' p
' ' ' p ' ' ' '
' u ' ' p ' ' ' ' ' ' B ' ' p ' p
Texture: -----
Artifacts:
838 (Hg)
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
ECKENFELDER INC. Contract: El Paso Energy -------------------
00050R
EPA SAMPLE NO.
W-16i
jb Name:
:Iii, Code: Case No.: _______ _ SAS No.: ________ SDG No.: 865/866(icp)
ltrix (soil/water ): __ w_a~t_e~r'---
Level (low/med):
'Solids:
Lab
Date
Sample ID: 98003125
Received: 05/07/98
I
I·
I
I
Concentration Units (ug/L or mg/kg dry weight): ug/L ---~"--C.....---
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I
' ' ' CAS No. lAnalyte
7429-90-5 Aluminum
7440-36-0 Antimony
7440-38-2 Arsenic
7440-39-3 Barium
7440-41-7 Beryllium
7440-43-9 Cadmium
--7440 70 2 ,Calcium
7440-47-3 !chromium
' 7440-48-4 :cobalt
' 7440-50-8 !Copper
7439-89-6 :Iron ' 7439-92-1 :Lead ' 7439-95-4 !Magnesium
7439-96-5 JManganese
7439-97-6 :Mercury
7440-02-0 !Nickel
7440-09-7 !Potassium
7782-49-2 :selenium
7440-22-4 Silver
7440-23-5 Sodium
7440-28-0 Thallium
7440-62-2 Vanadium
7440-66-6 ,Zinc
!cyanide ,_ ____ ..;
11
1
lor Before:
lier After: ----
Concentration
87.6
0.7
1.0
9.7
0.05
' 0.1 ' ' 910.6
1.6
0.2
1.1
157
' 0.4 ' ' 34.5 ' ' 1.0 ' ; 0.20
i 0.6
' 417.3 ' 1.0
0.2
51300
' 0.8 ' ' 7.0
5.6
clarity Befcre:
clarity After:
FORM I -IN
C Q M
B E p T
u p
u ' p ' B ' p ' ' '
' u ' p ' ' ' ' ' u ' p ' ' ' '
' B ' ' P,
B p
u p
B p
p
u ' p ' B p
B p
u cv;
' B p'
B p
B N p
u p
p
' u ' p ' ' ' ' ' B --' p '
B p
Texture: -----
Artifacts: -----
838 (Hg)
,,
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
00051R
EPA SAMPLE NO.
W-17s L'II Name: ECKENFELDER INC. Contract: El Paso Energy I _ _ccc.::..=:.;;.::;,,:_;=:;._:..________ ...::..::......:...::.::.::......:..=~.1.. _______ ___J
L!l Code: Case No.: SAS No.: SDG No.: 865/866(icp) ---------------Mtix (soil/water ): _ _::w~a~t~e~r;__
Level (low/med):
% 'lids:
Lab Sample ID: 98003126 _____ ....:__;_ __
Date Received: 05/07/98 _ __:c.::..:....:...:...c...::...::..___
I
Concentration Units (ug/L or mg/kg dry weight): ug/L ----"-'-----
I
t
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' ' ' 'CAS No. Analyte
7429-90-5 Aluminum
,7440-36-0 Antimony
:7440-38-2 ' '
Arsenic
:7440-33-3 Barium
!7440-41-7 Beryllium
! 7 440-43-9 Cadmium
0 7440-70-2 Calcium
7440-47-3 Chromium
7440-48-4 Cobalt
7440-50-8 Copper
7439-89-6 Iron
7439-92-1 Lead
7439-95-4 Magnesium
'7439-96-5 Manganese
7439-97-6 Mercury
7440-02-0 Nickel
7440-09-7 Potassium
7782-49-2 Selenium
7440-22-4 :silver
7440-23-5 !sodium
7440-28-0 !Thallium
7440-62-2 !vanadium
7440-66-6 !zinc
!cyanide -------
~l,.°r Before:
:!or A.:'ter:
I
Concentration
' 7380
0.7
1.0
953
1.0
0.1
223.8
6.3
45.5
30.0
1700
12.0
5350
494
0.36
23.8
' 4660
1.6
0.2
34900
' 1. 7 ' ' 1. 4 ' 174
clarity Before:
Clarity After:
FORM I -IN
' ' ' ' ' ' ' ' ' ' C Q M '
E p J
u p
u p
p
8 ' p ' u ' ' p ' ' 8 ' ' p ' ' 8 ' ' p ' ' B ' ' p ' ' ' ' p ' ' ' ' p ' ' ' ' p ' ' p
p
CV,
8 ' p '
8 p ' B N p i
u '., p ·, ' p
' 8 ' p
' ' ' 8 ' p ' ' p
Texture: ____ _
Artifacts: -----
838 ( Hg)
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I
U.S. EPA -CLP
1
00051AR
EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
L5JI Name: ECKENFELDER INC. Contract: El Paso Energy I FB5598
LI\ Code: Case No.: SAS No.: SDG No.: 865/866(icp) -----------------
Lab Sample ID: 98003127 ---------M.lrix ( soil/water ) : __ w_a_t_e_r __
Level (low/med): Date Received: 05/07/98 ---------
%1olids:
j
Concentration Units (ug/L or mg/kg dry weight): ug/L ----'-----
' I
' ' ' ICAS ' No. Analyte
' :
j7429-90-5 Aluminum
7440-36-0 Antimony
7440-38-2 Arsenic
7440-39-3 Barium
7440-41-7 Beryllium
7440-43-9 Cadmium
7440-70-2 Calcium
7440-47-3 Chromium
7440-48-4 Cobalt
:7440-50-8 Copper
' :7439-89-6 Iron
' i 7 439-92-1 Lead
7439-95-4 :-~agnesium
7439-96-5 Manganese
7 439-97-6 Mercury
\7440-02-0 Nickel
/7440-09-7 Potassium
!7782-49-2 Selenium
/7440-22-4 Silver
:7440-23-5 Sodium
7440-28-0 Thallium
7440-62-2 Vanadium
7440-66-6 Zinc
Cyanide i--------
11
lor Before:
lor After:
Concentration
' 8.7
0.7
_::.k{J /. i)
o.5
' 0.1 ' ' 0.1 ' ' 15.3 ' ' 0.3 ' ' 0.2 ' ' -Q.--&-(l, _; ' ' 6.2 ' ' ' 0.4
10.8
0.1
0.20
' 0.3
' 9.2
: 0. 6
' 0.2 ' ' 383.6 ' ' -,1-:"1 {'. t ' ' 0.2
0.5
Clarity Before:
Clarity After:
C Q
B E
u
.JYU
B
' B ' ' ' ' ' ' u ' ' ' ' ' ' B ' ' ' ' '
' u ' ' ' ' '
' u ' ' ' ' ' ' jl' j ' ' ' ' ' ' ' u ' ' ' ' ' ' ' u ' u ' ' B ' ' u
u
B
u N
u '. ' ' B ' ' ' ' .&·~ I./ I ' ' u ' u
Texture:
Artifacts:
' ' ' M ' ' ' ' !
Pi
Pj
p;
' p; ' p ' ' p ' ' p
p
p
p
' p ' p :
p ' ' p ' ' CV
p
p
p
p
p
p ' ' p ' p
---------
lmrnents:
I FORM I -IN
838 (Eg)
I
Nrune:
code:
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
00052R
EPA SAMPLE NO.
EB5598
ECKENFELDER INC. Contract: El Paso Energy -----------------=-=-...::..:;.::.:.....=..:=2.c:....J..._ ________ _j
Case No. : _______ _ SAS No.: ________ SDG No.: 865/866(icp)
838 (Hg)· ltrix (soil/water) : __ w_a_t_e_r __
Level (low/med):
Lab Sample ID: 98003128 ---------
Date Received: 05/07/98 _ ___:..:..;_.;..;..:...:..:. __
I solids:
I
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I
,I
Concentration Units (ug/L or mg/kg dry weight): ug/L ----''-'-----
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I
' ' ' 'CAS No.
7429-90-5
, 7440-36-0
!7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
' !7440-50-8
' 7439-89-6
7439-92-1
7439-95-4
!7439-96-5 ' !7439-97-6 ' !7440-02-0 ' :7440-09-7
!7782-49-2
!7440-22-4
:7440-23-5
!7440-28-0
!7440-62-2
:7 440-66-6
' ' '
li°lor Before:
lb1or After:
' ' ' 'Analyte
Aluminum
Antimony
!Arsenic
1Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
:Magnesium
!Manganese
!Mercury
Nickel
Potassium
Selenium
:silver
!sodium
!Thallium
!vanadium ' . : Zinc
!cyanide
----
lomrnents:
I
D
' ' ' : Concentration
' ' '
' !
' !
' ' ;
i
;
8.0
0.7
1.0
0.4
0.1
0.1
21.3
0.3
0.2
6.2
0.4
10.8
0.1
0.20
9.2
0.6
.. 0 .• 2 . ...
375.6
0.8
0.2
0.4
Clarity Before:
Clac·i ty After:
FORM I -IN
C Q M
E p ·< .J ' B
' u p
u p
p ' '
. u
p ' ' u
p u ' ' p B ' ' p u ' ' p u ' ' .. B-•'" 11 c· ' p
p u ' ' p ' u ' ' p ' u ' ' ' ' ! p B ' ' u ' ' !CV 1:,'.
Yr.' ' p
u ' p
u N : p
u ' ' ' p
' B p
u ' '
p
u .....
'
p
u p
,:
Texture: -----
Artifacts: -----
I
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APPENDIX F-4
DATA VALIDATION REPORT DATED
JANUARY 29, 1999
\ '\TN'\SYS\DAT A \l'ROJ\0313.08' ,l'DI-C\'R.DOC
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DAT A VALIDATION REPORT
FCX Statesville
Prepared By
Environmental Data Services, Ltd.
For
Eckenfelder, Inc.
January 29, 1999
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DATA ASSESSMENT NARRATIVES
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DATA ASSESSMENT NARRATIVE FOR VOLATILES
SITE: FCX Statesville
LABORATORY: Eckenfelder, Inc.
SAMPLE DELIVERY GROUP: FCX-V0817901
This sample delivery group consists of the following air samples:
111 B 7B 16B
Samples described above were analyzed via USEPA SW846 8260B to determine the concentration of
volatiles in air.
USEPA Contract Laboratory Program National Functional Guidelines for Organic Data Review (February
1994) have been considered during the validation of this data and in determining its usability.
All data are valid and acceptable except those analytes which have been qualified as described in the
attached glossary. All data qualification related to this group of samples is detailed on the attached
sheets.
Major Data Quality Issues
None.
Minor Data Quality Issues
Calibration -Two continuing calibrations had various compounds with percent difference values that
failed to meet validation criteria. The associated samples have the effected compounds qualified
as estimated.
Quantitation -Two samples had observed concentrations for tetrachloroethane reported based on an
instrument response over the calibration range. Therefore the results have been qualified as
estimated.
Two facts should be noted by all data users. First, the "R" flag means that the associated value is
unusable due to significant QC problems, the data is invalid and provides no information as to whether
the compound is present or not. "R" values should not appear on any data tables even as a last resort.
Lastly, strict QC serves to increase confidence in data but any value potentially contains error.
/
(
chmidt
Environmental ScientisUDirector
Date:
1
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HOLDING TIME
The amount of an analyte can change with time due to chemical instability, degradation, volatilization, etc. If the specified holding time is exceeded the data may not be valid.
The analyses performed on samples in this sample delivery group were all done within established holding times.
BLANK CONTAMINATION
Quality assurance blanks, method, trip, field, or rinse blanks are prepared to identify any contamination which may have been introduced into the samples during preparation or field activity. Method blanks measure lab contamination. Trip blanks measure cross contamination during shipment. Field and rinse blanks measure cross contamination during field operations.
Method Blank Contamination
Method blanks were analyzed at the proper frequency. Upon examination, the method blanks did not contain any target analyte at or above reportable concentration levels.
MASS SPECTROMETER TUNING
Tuning and performance criteria are established to ensure adequate mass resolution, proper identification of compounds, and to some degree, sufficient instrument sensitivity. These criteria are not sample specific. Instrument performance is determined using standard materials. Therefore, these criteria should be met in all circumstances.
The tuning standard for volatiles is bromofiuorobenzene (BFB).
All of the instrument tunes associated with this SDG were fully compliant.
CALIBRATION
Satisfactory instrument calibration is established to ensure that the instrument is capable of producing acceptable quantitative results. The initial calibration curve demonstrates that the instrument is capable of giving acceptable performance at the beginning of an analytical sequence. The continuing calibration verifies that the instrument is giving satisfactory daily performance.
Response Factor
The response factor measures the instruments responses to specific chemical compounds. The response factors for the VOA Target Compound List must be greater than or equal to 0.05 in both the initial and continuing calibrations. A value less than 0.05 indicates serious detection and quantitation problems.
RRF values in all initial and continuing calibrations were greater than 0.05.
2
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,o
Percent Relative Standard Deviation (RSD) and Percent Deviation (%D)
'
Percent RSD is calculated from tJe initial calibration and is used to indicate stability of a specific
compound over the calibration range. %D compares the response factor of the continuing calibration with
the mean response factor of the initial calibration. Therefore %Dis a measure of the instruments daily
perfonmance.
The following QC criteria has been applied for this project:
% RSD of initial calibration must be <30.0 %
% D for continuing calibrations must be <25.0%
A value outside these limits indicates potential detection and quantitation errors. According to USEPA
CLP National Functional Guidelines for Organic Data Review (2194), all positive and non-detect results
are flagged as estimated.
The initial and continuing calibrations associated with this sample delivery group met all validation criteria
with the following exceptions.
The continuing calibration perfonmed on 8/27 /98 had an observed percent difference for 1,2-dibromo-3-
chloropropane (28. 7%) that exceeded validation criteria. The following samples were associated with the
above calibration.
I 3A I 4A
All samples were non-detected for the effected compound and have been qualified as estimated (UJ).
The continuing calibration perfonmed on 8/28/98 failed to meet the validation criteria for the compounds
listed below.
acetone 144.0%
2-butanone 96.2%
1,2-dibromo-3-chloropropane 31.9%
hexanone 61.1 %
methylene chloride 29.5%
The following samples were associated with the above calibration_.
11 18 I 5B I 2B I 6B I 7B 11
All samples were non-detected for the effected compounds and have been qualified as estimated (UJ).
3
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INTERNAL STANDARDS PERFORMANCE
Internal standard performance criteria is meant to ensure that the GC/MS sensitivity and response are
stable during every experimental run.
The internal standard area count must not vary by more than a factor of two from the associated
continuing calibration standard. The retention time of the internal standard must not vary by more than+/-
30 seconds from the associated continuing calibration standard. If the area count is outside the (-50% -
100%) range of the associated standard, all positive results for compounds quantitated using that
standard are qualified as estimated, and non detects as UJ, but only if area is< 50%.
Internal standard recoveries observed in all samples and method blanks were within acceptable limits.
SURROGATES
All samples and blanks are spiked with surrogate compounds prior to sample preparation and analyses to
evaluate overall laboratory performance and efficiency of the analytical technique.
All samples and method blanks evaluated in this report had observed surrogate recoveries within the
established limits.
COMPOUND IDENTIFICATION
Volatile
TCL compounds are identified on the GC/MS by using the analyte's relative retention time (RRT) and ion
spectra. For the results to be a positive hit, the sample peak must be within :t 0.06 RRT units of the
standard compound, and have an ion spectra which has a ratio of the primary and secondary ion
intensities within 20% of that in the standard compound. No analytes were qualified for compound
identification.
Tetrachloroethene results for samples 1 Band 2A were reported based on an instrument signal that was
over the calibration range. The air sample matrix limits the laboratory to one analysis per sample.
Therefore, no diluted analyses could be performed and the effected results have been qualified as
estimated.
MATRIX SPIKE/MATRIX SPIKE DUPLICATE
The matrix spike and matrix spike duplicate are generated to determine the precision and accuracy of the
analytical procedure in a given matrix. This information may be used to qualify data.
A matrix spike/matrix spike duplicate determination is not applicable to air samples. No matrix specific
evaluation of precision or accuracy can be performed.
Laboratory control samples were processed at a frequency of one per twelve hour analysis period. LCS
recoveries were well within acceptance limits in every case with the following exception. Laboratory
control sample 8/28/98 had an observed percent recovery for vinyl chloride (160%) above the upper QC
limit (140%). No qualification of data was performed based on this parameter since vinyl chloride was net
positively identified in any associated sample.
4
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OTHER QC DATA OUT OF SPECIFICATION
None.
FIELD DUPLICATE
No field duplicate was identified within this delivery group. No field precision evaluation was made.
SYSTEM PERFORMANCE AND OVERALL ASSESSMENT
Non-compliant continuing calibration percent difference values were found to impact the results reported.
All other QC criteria appears to be acceptable.
5
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DATA ASSESSMENT NARRATIVE FOR VOLATILES
SITE: FCX Statesville
LABORATORY: Eckenfelder, Inc.
SAMPLE DELIVERY GROUP: FCX-V0819401
This sample delivery group consists of the following water samples:
MP-2B (B-14-98) MP-2C (B-14-98) MP-20 (B-14-98) MP-1B (B-14-98)
MP-1D 18-14-98) MP-3C 18-14-98) MP-3D fB-14-98) MP-4B fB-14-98\
MP-4D (B-14-98) MP-SB (B-14-98) MP-SC (8-14-98) MP-SD (8-14-98)
AS-1 18-19-98\ AS-2 18-19-98\ AS-2 DUP 18-19-98\ W-20D 122'
Trip Blank 106811070 MP-1C (B-27-98) MP-2C (B-27-98) MP-3C (B-27-98)
MP-SC (B-27-98) AS-2 (B-27-98) AS-1 /8-27-98) MP-3B (8-28-98)
MP-2B (B-28-98) Trip Blank 1085/1086 MP-1 B (B-28-98)
MP-1C (8-14-98)
MP-4C 18-14-98\
Trip Blank 106811069
W-20D 142'
MP-4C (B-27-98)
MP-3D [B-28-98)
Samples described above were analyzed via US EPA Low Level CLP SOW OLC01 .0 to determine the
concentration of volatiles in water.
US EPA Contract Laboratory Program National Functional Guidelines for Organic Data Review (February
1994) have been considered during the validation of this data and in determining its usability.
All data are valid and acceptable except those analytes which have been qualified as described in the
attached glossary. All data qualification related to this group of samples is detailed on the attached
sheets.
Major Data Quality Issues
None.
Minor Data Quality Issues
Blank Contamination -Various common laboratory contaminants were present in method and trip blanks
associated with samples in this delivery group. Effected compound results have been qualified
per USEPA guidelines.
Calibrations -Several continuing calibrations had compounds with observed percent difference values
that failed to meet validation criteria. The associated samples have the effected compounds
qualified as estimated.
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HOLDING TIME
The amount of an analyte can change with time due to chemical instability, degradation, volatilization, etc.
If the specified holding time is exceeded the data may not be valid.
The analyses perfonmed on samples in this sample delivery group were all done within established
holding times.
BLANK CONTAMINATION
Quality assurance blanks, method, trip, field, or rinse blanks are prepared to identify any contamination
which may have been introduced into the samples during preparation or field activity. Method blanks
measure lab contamination. Trip blanks measure cross contamination during shipment. Field and rinse
blanks measure cross contamination during field operations.
Method Blank Contamination
Method blanks were analyzed at the proper frequency. Upon examination, the method blanks did not
contain any target analyte at or above reportable concentration levels with the following exception:
The method blank analyzed on 8/18/98 (V1 BLK0818) was found to contain acetone at a concentration of
1.5 ppb. Sample MP-4D 8/14/98 was associated with the method blank described above.
Larger amounts of acetone were found in trip blank 1068/1069 associated with the MP-4D sample.
Therefore the acetone value was qualified based on the amount of acetone found in trip blank 1068/1069.
Field Blank/Trip Blank Contamination
Three trip blanks and a storage blank were analyzed in association with the samples in this delivery
group. Concentrations of contaminants observed in the blanks are listed below.
Blank
Trip Blank 1068/1069
Trip Blank 1068/1070
Trip Blank 1085/1086
Storage Blank
Acetone
2.0 ppb
2.3 ppb
3.4 ppb
1.8 ppb
Methylene Chloride
2.1 ppb
2.2 ppb
1.0 ppb
1.2 ppb
Per validation guidelines samples associated with the blanks described above were qualified based on
the highest concentration blank.
Acetone (3.4 ppb) and methylene chloride (1.0 ppb) were found in trip blank 1085/1086. The following
samples were associated with trip blank 1085/1086 and contained the contaminants in the effected
concentration range:
Ii AS-1 / AS-2 I MP-1C / MP-3D
The effected sample results for the samples listed above have been qualified "U" as appropriate.
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Trip blank 1068/1070 contained acetone (2.3 ppb) and methylene chloride (2.2 ppb). The following
samples were association with trip blank 1068/1070 and contain the contamiants in the effected
concentration range.
Ii W-20D 122 fl. \ W-20D 142 fl. I AS-2 Duplicate
The effected sample results for the samples listed above have been qualified "U" as appropriate.
Trip blank 1068/1069 contained acetone (2.0 ppb) and methylene chloride (2.1 ppb). The samples listed
below were associated with trip blank 1068/1067 and contain the contaminants in the effected
concentration range.
MP-3D MP-3C MP-4C MP-1D MP-2D
MP-1C MP-4B MP-5B MP-4D MP-2C
The effected sample results for the samples listed above have been qualified "U" as appropriate.
MASS SPECTROMETER TUNING
Tuning and performance criteria are established to ensure adequate mass resolution, proper identification
of compounds, and to some degree, sufficient instrument sensitivity. These criteria are not sample
specific. Instrument performance is determined using standard materials. Therefore, these criteria should
be met in all circumstances.
The tuning standard for volatiles is bromofiuorobenzene (BFB).
All instrument tunes associated with this SDG were fully compliant.
CALIBRATION
Satisfactory instrument calibration is established to ensure that the instrument is capable of producing
acceptable quantrtative results. The initial calibration curve demonstrates that the instrument is capable of
giving acceptable performance at the beginning of an analytical sequence. The continuing calibration
verifies that the instrument is giving satisfactory daily performance.
Response Factor
The response factor measures the instruments responses to specific chemical compounds. The response
factors for the VOA Target Compound List must be greater than or equal to 0.05 in both the initial and
continuing calibrations. A value less than 0.05 indicates serious detection and quantitation problems.
RRF values in all initial and continuing calibrations were greater than 0.05.
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Percent Relative Standard Deviation (RSD) and Percent Deviation (¾D)
Percent RSD is calculated from the initial calibration and is used to indicate stability of a specific
compound over the calibration range. %D compares the response factor of the continuing calibration with
the mean response factor of the initial calibration. Therefore %D is a measure of the instruments daily
performance.
The following QC criteria has been applied for this project:
% RSD of initial calibration must be <30.0 %
% D for continuing calibrations must be <25.0%
A value outside these limits indicates potential detection and quantitation errors. According to USEPA
CLP National Functional Guidelines for Organic Data Review (2194), all positive and non-detect results
are flagged as estimated.
The initial and continuing calibrations associated with this sample delivery group met all validation criteria
with the following exceptions. The initial calibration performed on 5/11 /98 0/OA 1) had an observed %
RSD value for bromoform (30.4%) that exceeded validation acceptance limit. No associated sample
analyses yielded a positive value for bromoform. Therefore no qualification of data was necessary.
The continuing calibration performed on (8-18-98) had observed percent difference values for carbon
disulfide (32.1%) and chloromethane (45.7%) that exceeded validation criteria. Samples MP-4D and !lip
blank (1068 & 1069) were associated with the above non-compliant calibration. Carbon disulfide and
chloromethane were non-detected in both samp_les and results have been qualified as estimated (UJ).
The continuing calibration performed on (8-19-98) had an observed percent difference values for
chloromethane (39. 7%) that exceeded validation criteria. The following samples were associated with the
above calibration.
II MP-2B I MP-2C I MP-20 I MP-18 I MP-1C I MP-1D I MP-5B
All samples were non-detected for the effected compound and have been qualified as estimated (UJ).
The continuing calibration performed on (8-24-98) had observed percent difference values for carbon
disulfide (31.2%), chloromethane (34.3%) and 1,2-dibromo-3-chloropropane (26.7%) that exceeded
validation criteria. The following samples were associated with the above calibration.
II Trip Blank 106811070 I AS-1 I W-20D 122' I W-20D 142' I MP-SC I MP-5D II
All samples were non-detected for the effected compounds and have been qualified as estimated (UJ).
The continuing calibration performed on (8-25-98) had observed percent difference values for carbon
disulfide (33.2%), chloromethane (54.2%) and 1,2-dibromo-3-chloropropane (30.2%) that exceeded
validation criteria. The following samples were associated with the above calibration.
AS-2 MP-4B MP-3C
MP-3D MP-4C AS-2 DUP Stora e Blank
All samples were non-detected for the effected compounds and have been qualified as estimated (UJ).
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The continuing calibration (9-3-98) had an observed percent difference values for ch\oromethane (31.3%)
that exceeded validation criteria. The following samples were associated with the above non-compliant
calibration.
II MP-2C I MP-3C I MP-4C I MP-SC I MP-1C I Trip Blank 1085/1086 II
All samples were non-detected for the effected compounds and have been qualified as estimated (UJ).
The continuing calibration (9-4-98) had observed percent difference values for chloromethane (34.3%)
and 1,2-dibromo-3-chloropropane (28.5%) that exceeded validation criteria. The following samples were
associated with the above non-compliant calibration.
II MP-38 I MP-3O I MP-28 I MP-18 I AS-2 I AS-1
All samples were non-detected for the effected compounds and have been qualified as estimated (UJ).
INTERNAL STANDARDS PERFORMANCE
Internal standard perfonnance criteria is meant to ensure that the GC/MS sensitivity and response are
stable during every experimental run.
The internal standard area count must not vary by more than a factor of two from the associated
continuing calibration standard. The retention time of the internal standard must not vary by more than +/-
30 seconds from the associated continuing calibration standard. If the area count is outside the (-50% -
100%) range of the associated standard, all positive results for compounds quantitated using that
standard are qualified as estimated, and non detects as UJ, but only if area is< 50%.
Internal standard recoveries observed in all samples and method blanks were within acceptable limits.
SURROGATES
All samples and blanks are spiked with surrogate compounds prior to sample preparation and analyses to
evaluate overall laboratory perfonnance and efficiency of the analytical technique.
All samples and method blanks evaluated in this report had observed surrogate recoveries within the
established limits.
COMPOUND IDENTIFICATION
Volatile
TCL compounds are identified on the GC/MS by using the analyte's relative retention time (RRT) and ion
spectra. For the results to be a positive hit, the sample peak must be within± 0.06 RRT units of the
standard compound, and have an ion spectra which has a ratio of the primary and secondary ion
intensities within 20% of that in the standard compound. No analytes were qualified for compound
identification.
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MATRIX SPIKE/MATRIX SPIKE DUPLICATE
The matrix spike and matrix spike duplicate are generated to determine the precision and accuracy of the
analytical procedure in a given matrix. This information may be used to qualify data.
Sample W-20D 122 ft. was analyzed as matrix spike. Upon evaluation all accuracy indicators were
favorable. No significant matrix interferences were apparent.
Laboratory control samples were processed at a frequency of one per twelve hour analysis period. LCS
recoveries were well within acceptance limits in every case.
OTHER QC DATA OUT OF SPECIFICATION
None.
FIELD DUPLICATE
Samples AS-2 and AS-2 DUP comprise the field duplicate pair associated with samples in this delivery
group. Field precision exhibited was extremely good. The largest percent difference observed for
positively identified target analytes between the pair was less than 15%. Field precision was
demonstrated to be well within acceptable tolerances.
SYSTEM PERFORMANCE AND OVERALL ASSESSMENT
Non-compliant continuing calibrations and control blank contamination were found to impact the results
reported. All other QC criteria appears to be acceptable.
Note: The data collected listed on the "storage blank" form I is 8/29/98 while the date analyzed is
8/25/98. This anomaly should be investigated and corrected if possible.
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LABORATORY DATA WITH QUALIFIERS ADDED
000-1-6
FORM 1 CLIENT SAMPL~ Nv.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lA
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
11Jb Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0817901
~trix: (soil/water) AIR Lab Sample ID: 9808179-01
tmple
Level:
wt/vol:
(low/med)
5.000 (g/mL) ML
LOW
Lab File ID:
Date Sampled:
0817901D
08/25/98
11Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
lil Extract Volume : _____ (uL)
Date Analyzed: 08/27/98
Dilution Factor: 1.0
Soil Aliquot Volume:
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4 -

-

-

-

-

-

-

-
-Br·omochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-i--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-1,2-Dichloroethene
156-60-5--------trans-1,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-1,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __ l
FORM I VOA
50 u
10 u
10 u
10 u
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20 u
100 u
10 u
10 u
10 u
20 u
10 u
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10 u
10 u
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10 u
10 u
10 u
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10 u
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10 u
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[! J
00017
FORM 1 CLIENT SAMPLE NO. ~
VOLATILE ORGANICS ANALYSIS DATA SHEET
lA
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
gab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0817901
latrix: (soil/water) AIR
uample
Level:
wt/vol:
(low/med)
I Moisture: not dee.
5.000 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
loil Extract Volume : ____ (uL)
Lab Sample ID: 9808179-01
Lab File ID:
Date Sampled:
0817901D
bB/25/98
Date Analyzed: 08/27/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene 150
108-88-3--------Toluene 10 u
71-55-6---------1,1,1-Trichloroethane 10 u
79-00-5---------1,1,2-Trichloroethane 10 u
79-01-6---------Trichloroethene 10 u
75-01-4---------Vinyl chloride 20 u
1330-20-7-------Xylene(total) 10 u
FORM I VOA
eeH:)22 D FORM 1 CLIENT SAMI-.u,, "u.
VOLATILE ORGANICS ANALYSIS DATA SHEET
0 2A gab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Lab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0817901
Oatrix: (soil/water) AIR Lab Sample ID: 9808179-02
"'ample wt/vol:
Uevel: (low/med)
IJ Moisture: not dee.
5. 000 (g/mL) ML
LOW
le Column: DB-624 ID: 0.53 (mm)
Lab File ID: 817902D2
Date Sampled: 08/25/98
Date Analyzed: 08/27/98
Dilution Factor: 1.0
.oil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (uL)
CONCENTRATION UNITS:
CAS NO.
I
COMPOUND (ug/L or ug/Kg) UG/L . Q
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67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulb.de
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1------~-Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
50 u
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10 u
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100 u
10 u
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10 u
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10 u -
10 u
10 u
0
u 00023
FORM 1 CLIENT SAMPLE-No1
• •v
a VOLATILE ORGANICS ANALYSIS DATA SHEET
2A
Lab Name: ECKENFELBER INC. Contract: EL PASO ENERGY
1lt Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0817901
Matrix: (soil/water) AIR
.ple wt/vol: 5.000 (g/mL) ML
Level: (low/med) LOW
••Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm) lil Extract Volume : ____ (uL)
Lab Sample ID: 9808179-02
Lab File ID: 817902D2
Date Sampled: 08/25/98
Date Analyzed: 08/27/98
Dilution Factor: 1.0
Soil Aliquot Volume:
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene 240 E
108-88-3--------Toluene 10 u
71-55-6---------1,1,1-Trichloroethane 10 u
79-00-5---------1,1,2-Trichloroethane 10 u
79-01-6---------Trichloroethene 10 u
75-01-4---------Vinyl chloride 20 u
1330-20-7-------Xylene(total) 10 u
FORM I VOA
00028 0 FORM 1 CLIENT SAMPLE-N0° .• -VOLATILE ORGANICS ANALYSIS DATA SHEET
u Lab Name: ECKENF.ELDER INC. Contract: EL PASO ENERGY
3A
Lab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0817901
UMatrix: (soil/water) AIR Lab Sample ID: 9808179-03
Sample wt/vol: 2.500 (g/mL) ML Lab File ID: 0817903D I Lev.el: (low/med) LOW Dat·e Sampled: 08/25/98 u %-Moisture: not dee.
GC Column: DB-624 ID: 0. 53 (mm)
Date·Analyzed: 08/27/98
Dilution Factor: 1.0 I Soil Extract Volume : ____ (uL) Soil Aliquot Volume: ____ (uL)
g
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CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
67-64-1---------Acetone 100 u 71-43-2---------Benzene 20 u 75-27-4---------Bromochloromethane 20 u 75-27-4---------Bromodichloromethane 20 u 75-25-2---------Bromoform 20 u 74-83-9---------Bromomethane 40 u 78-93-3---------2-Butanone 200 u 75-15-0---------Carbon disulfide 20 u 56-23-5---------Carbon tetrachloride 20 u 108-90-7--------Chlorobenzene 20 u 75-00-3---------Chloroethane 40 u 67-66-3---------Chloroform 20 u 74-87-3---------Chloromethane 40 u 124-48-1--------Dibromochloromethane 20 u 96-12-8---------1,2-Dibromo-3-chloropropane 20 u 106-93-4--------1,2-Dibromoethane -20 u 95-50-1---------1,2-Dichlorobenzene 20 u 541-73-1--------1,3-Dichlorobenzene 20 u 106-46-7--------1,4-Dichlorobenzene 20 u 75-34-3---------1,1-Dichloroethane 20 u 107-06-2--------1,2-Dichloroethane 20 u 75-35-4---------1,1-Dichloroethene 20 u 156-59-2--------cis-l,2-Dichloroethene 20 u 156-60-5--------trans-l,2-Dichloroethene 20 u 78-87-5---------1,2-Dichloropropane --20 u 10061-01-5-----~cis-l,3-Dichloropropene 20 u 10061-02-6------trans-l,3-Dichloropropene 20 u 100-41-4--------Ethylbenzene --20 u 591-78-6--------2-Hexanone 20 u 75-09-2---------Methylene chloride 20 u 108-10-1--------4-Methyl-2-pentanone 20 u -100-42-5--------Styrene 20 u 79-34-5---------1,1,2,2-Tetrachloroethane 20 u --
FORM I VOA
0 r00029
FORM 1 CLIENT SAMPL-
VOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: ECKENFELBER INC. Contract: EL PASO ENERGY
3A
gab ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0817901
latrix: (soil/water) AIR
gample wt/vol:
Level: (low/med) g Moisture: not dee.
2.500 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm) loil Extract Volume: ____ (uL)
CAS NO. COMPOUND
Lab Sample ID: 9808179-03
Lab·File ID: 0817903D
Date Sampled: 08/25/98
Date Analyzed: 08/27/98
Dilution Factor: 1.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
----
Q
127-18-4--------Tetrachloroethene _____ _ 140
20 U
20 U
20 U
20 U
40 U
20 U
108-88-3--------Toluene 71-55-6---------1,1,1-T_r_i_c~h-l~o-r_o_e_t~h-a_n_e ___ _
79-00-5---------1,1,2-Trichloroethane ___ _
79-01-6---------Trichloroethene -------75-01-4---------Vinyl chloride ______ _
1330-20-7-------Xylene(total) _______ _
(uL)
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···-·-·--·-·-·----
FORM I VOA
I FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
4A
Name: ECKENFELgER INC. Contract: EL PASO ENERGY
Ijb ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0817901
tltrix: (soil/water) AIR
IJmple
i!Jvel:
wt/vol:
(low/med)
2.500 (g/mL) ML
LOW
'Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808179-04
Lab File ID:
Date Sampled:
0817904
08/25/98
Date Analyzed: 08/27/98
Dilution Factor: 1.0
fil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4-c-------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloricte
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichlc~oethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10~1-----0 -0 4 0 Methyl::.2::p~nta11,Q11e
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetracnloroethane __
FORM I VOA
Q
100 u
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20 u
20 u
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200 u
20 u
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20 u
40 u
20 u
20 u u :r
20 u
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I
lab
FORM 1
OOO?fl-
cLIENT SAMPLE; J\lo'.-
VOLATILE ORGANICS ANALYSIS DATA SHEET
4A
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
1ab ~ode: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0817901
'1atrix: (soil/water) AIR Lab Sample ID: 9808179-04
lample
Level:
wt/vol:
(low/med)
2.500 (g/mL) ML
LOW
Lab File ID:
Date Sampled:
0817904
08/25/98
I Moist_ure: not dee. Date Analyzed: 08/27/98
Dilution Factor: 1.0 GC Column: DB-624 ID: 0. 53 (mm)
loil Extract Volume : ____ (uL) Soil Aliquot Volume: ____ (uL)
I
n
0
u
g
I
I
•
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene
108-88-3--------Toluene ------
71-55-6---------1,l,l-Trichloroethane
79-00-5---------1,l,2-Trichloroethane ----
79-01-6---------Trichloroethene ----
75-01-4---------Vinyl chloride --------1330-20-7-------Xylene(total) _______ _
FORM I VOA
120
20 U
20 U
20 U
20 U
40 U
20 U
Q
-000-38
FORM 1 CLIENT SAMPL~ NU.
VOLATILE ORGANICS ANALYSIS DATA SHEET
1B
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
)fb Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0817901
,filatrix: (soil/water) AIR
tmple
Level:
wt/vol:
(low/med)
OMoisture: not dee.
5.000 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808179-08
Lab File ID:
Date Sampled:
0817908
08/25/98
Date Analyzed: 08/28/98
Dilution Factor: 1.0
~il Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (uL)
0
D
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disult1.de
56-23-5---------Carbon tetrachlor1.ae
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane -106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-1,2-Dichloroethene
156-60-5--------trans-1,2-Dichloroethene --78-87-5---------1,2-Dichloropropane
10061-01-5------cis-1,3-Dichloropropene
10061-02-6------trans-1,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
50
10
10
10
10
20
100
10
10
10
20
10
20 io
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
108-10-1--------4-Methyl-2-pentanone .. --·--. ·-----------10
100-42-5--------Styrene 10
79-34-5---------1,1,2,2-Tetracnloroethane --10
FORM I VOA
Q
u u
u u
u
uf u
u
u u
u u
u u
u
u
u
u
u
u
u u
u u u u
u
u u
u u ' }J
-U----u u
...Q.0_03_9
CLIENT SAMPLE NO. FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
lB
ECKENFELDER INC. Contract: EL PASO ENERGY
r-b Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0817901
Matrix: (soil/water) AIR
ft-mple wt/vol: 5.000 (g/mL) ML
Level: (low/med) . LOW
10, Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808179-08
Lab File ID: 0817908
Date Sampled: 08/25/98
Date Analyzed: 08/28/98
Dilution Factor: 1.0
lloil Extract Volume : ____ (uL) Soil Aliquot Volume: ____ (uL)
0
i
I
I!
i
'I
i
I
I
i
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene _____ _
108-88-3--------Toluene 71-55-6---------1,1,1-T_r_i_c~h~r-o_r_o_e_t~hra~n-e ___ _
79-00-5---------1,1,2-Trichloroethane ___ _
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride-------
1330-20-7-------Xylene(total) _______ _
FORM I VOA
210 E
10 U
10 U
10 U
10 U
20 U
10 U
Q
/ J
I FORM 1
00043
CLIENT SAMPLE.NO:
VOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: ECKENFELfl:ER INC. Contract: EL PASO ENERGY
2B
1tb Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0817901
Matrix: (soil/water) AIR
ff-mple wt/vol: 2.500 (g/mL) ML
Level: (low/med) LOW
d"Moisture: not dee.
GC Column: DB-624 ID: 0. 53 (mm)
Lab Sample ID: 9808179-09
Lab File ID:
Date Sampled:
817909D2
08/25/98
Date Analyzed: 08/28/98
Dilution Factor: 1.0
Soil Aliquot Volume: lil Extract Volume : _____ (uL) -----,-,. ,,
I
-Ill I
I ,,
I
1·
j ,.
·1
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L .
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulride
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-1,2-Dichloroethene
156-60-5--------trans-1,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-1,3-Dichloropropene
10061-02-6------trans-1,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Eexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone -
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __ l
FORM I VOA
100
20
20
20
20
40
200
20
20
20
40
20
"10
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u
Q
··--··-·
u:r
uJ
v':f
uJ . ., ,,
(uL)
00044
FORM 1 CLIENT SAMPL_
VOLATILE ORGANICS ANALYSIS DATA SHEET
2B
Name: ECKENF£LBE-R INC. Contract: EL PASO ENERGY lb Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0817901
~atrix: (soil/water) AIR
tmple wt/vol:
Level: (low/med)
'Moisture: not dee.
2.500 (g/mL) ML
LOW
GC Column: DB-624 ID: 0. 53 (mm)
'il Extract Volume: ____ (uL)
Lab Sample ID: 9808179-09
Lab File ID: 817909D2
Date Sampled: 08/25/98
Date Analyzed: 08/28/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
I
11,
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
,1\
·I
I·
i
I
I
I
I
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
170
20 u
20 u
20 u
20 u
40 u
20 u
FORM 1
,00.Q48 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SB
Name: ECKENFELQER INC. Contract: EL PASO ENERGY
Tlb ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0817901
. trix: (soil/water) AIR Lab Sample ID: 9808179-12
I. mple
vel:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
Lab File ID:
Date Sampled:
0817912
08/25/98
·1 Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm) til Extract Volume: ____ (uL)
Date Analyzed: 08/28/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
\I·
1·
I
I
·I -.:
I
.I
I ,.
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-1---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloriae
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene --78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
... 108~10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
Q
10 u
2.0 u
2.0 u
2.0 u
2.0 u
4.0 u
20 u
2.0 u
2.0 u
2.0 u
4.0 u
2.0 u
4.0 u
2:0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
.2 . 0 u
2.0 u
2.0 u
'
00049
FORM 1 CLIENT SAMPLE Nu.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SB
Name: ECKEN~EL~ER INC. Contract: EL PASO ENERGY
l b ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0817901
trix: (soil/water) AIR
rmple
!level:
wt/vol:
(low /med) I Moisture: not dee.
25.00
LOW
(g/rnL) ML
GC Column: DB-624 ID: 0.53 (mm)
til Extract Volume: ____ (uL)
Lab Sample ID: 9808179-12
Lab File ID:
Date Sampled:
0817912
08/25/98
Date Analyzed: 08/28/98
Dilution Factor; 1.0
Soil Aliquot'volume: ----
t ,,,
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I
I
' I
I
i
I
I
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,i,l-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
1. 2 J
2.0 u
2.0 u
2.0 u
2.0 u
4.0 u
2.0 u
(uL)
I FORM 1 CLIENT SAMPLE9Po·?_!il3
VOLATILE ORGANICS ANALYSIS DATA SHEET
6B
Name: ECKENFELBER INC. Contract: EL PASO ENERGY
Ijb Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0817901
tltrix: (soil/water) AIR
I-.mple
vel:
wt/vol:
(low/med)
fMoisture: not dee.
2.500 (g/mL) ML
LOW
I: Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808179-13
Lab File ID:
Date Sampled:
0817913D
08/25/98
Date Analyzed: 08/28/98
Dilution Factor: 1.0
lil Extract Volume: _____ (uL) ,Soil Aliquot Volume: ____ (uL)
i ,.,.
·I
I
I
i
·I
i
I
i
' I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane -106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene --78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
100
20
20
20
20
40
200
20
20
20
40
20
40
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
_20
20
20
u u
u
u
u
u u u
u u
u u
u u
u
u
u
u
u
u u u
u u
u u u u u
u
u
u
u
Q
"
,-cJ
FORM 1
JWQ.5_9
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
6B
Name: ECKENFELBER INC. Contract: EL PASO ENERGY
l b Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0817901
,e;.trix: (soil/water) AIR
f-mole
~evel:
wt/vol:
(low/med) I Moisture: not dee.
2.500
LOW
(g/mL) ML
GC Column: DB-624 ID: 0.53 (mm)
til Extract Volume: ____ (uL)
Lab Sample ID: 9808179-13
Lab File ID:
Date Sampled:
0817913D
08/25/98
Date Analyzed: 08/28/98
Dilution Factor: 1.0
Soil Aliquot Volume: ----
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
'
I
I
I
I
I
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroetnane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
110
20 u
20 u
20 u
20 u
40 u
20 u
(uL)
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
7B
Name: ECKENFELIBR INC. Contract: EL PASO ENERGY
L';i' ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX;V0817901
M.rix: (soil/water) AIR
Siple
L iel:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
~,-oisture: not dee.
G Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808179-14
Lab File ID:
Date Sampled:
0817914
08/25/98
Date Analyzed: 08/28/98
Dilution Factor: 1.0
1-1 Extract Volume: (uL) ----Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
'I
-g,
ff
a
u
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--~-----Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106~46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene cnloride
108-10-1:: -::.c: .c_-...= 4-MethyL:2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane -1
FORM I VOA
Q
10 u
2.0 u
2.0 u
2.0 u
2.0 u
4.0 u
20 u
2.0 u
2.0 u
2.0 u
4.0 u
2.0 u
0.79 J
2.0 u
2.0 u /)J
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u
2.0 u ,./ J
2.0 u
2.0 u
I
lb
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELBER INC. Contract: EL PASO ENERGY
7B
,Jiiab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0817901
latrix: (soil/water) AIR
lample
..,evel:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
Lab
Lab
Date
Date
Sample ID: 9808179-14
File ID: 0817914
Sampled: 08/25/98
Analyzed: 08/28/98 jcMoisture: not dee.
~ Column: DB-624 ID: 0.53 (mm) Dilution Factor: 1.0
toil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
' I
I
I
I,
·1
I,
I
I
I,
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene
108-88-3--------Toluene ------
71-55-6---·------l,l,l-Trichloroethane
79-00-5---------1,l,2-Trichloroethane ----
79-01-6---------Trichloroethene ----
75-01-4---------Vinyl chloride --------1330-20-7-------Xylene(total) _______ _
FORM I VOA
16
2.0 U
2. 0 U
2. 0 U
2.0 U
4.0 U
2.0 U
Q
'I FORM 1
00052
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
'ab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
MP-2B
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix: (soil/water) WATER Lab Sample ID: 9808092-01
I ample wt/vol: Lab File ID: 809201D2
Level: (low/med) I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0. 53 (mm)
Date Sampled: 08/14/98
Date Analyzed: 08/19/98
Dilution Factor: 25.0
loil Extract Volume: _____ (uL) Soil Aliquot Volume:
1
I
I
I
I
I
I
!I
I
I
I
i
I
.
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-1,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-1,3-Dichloropropene
10061-02-6------trans-1,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
120
25
25
25
25
25
120
25
25
25
25
25
.25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
120
so
120
25
25
____ (uL)
Q
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
I
I
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
00053
CLIENT SAMPLE NO.
MP-2B
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
.b Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix: (soil/water) WATER
lample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW
I Moisture: not dee.
r,C Column: DB-624 ID: 0. 53 (mm)
■oil Extract Volume: (uL) ----
Lab Sample ID: 9808092-01
Lab File ID: 809201D2
Date Sampled: 08/14/98
Date Analyzed: 08/19/98
Dilution Factor: 25.0
Soil Aliquot Volume: ____ (uL)
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
' I
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
350 D
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
I 00058
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
'ab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
MP-2C
Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix:
lample
(soil/water) WATER
wt/vol:
Level: (low/med) 0 Moisture: not dee.
25. 00 (g/mL) ML
LOW
Lab
Lab
Date
Date
Sample ID: 9808092-02
File ID: 809202D2
Sampled: 08/14/98
Analyzed: 08/19/98
GC Column: DB-624 ID: 0. 53 (mm) Dilution Factor: 50.0
Moil Extract Volume: (uL) -----Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulb.de
56-23-5---------Carbon tetrachlon.de
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
1200
50
50
50
50
50
250
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
250
75-09-2---------Methylene chlon.de I ClC,-4-r-
108-10-1--------4-Methyl-2-pentanone 250
100-42-5--------Styrene 50
79-34-5---------1,1,2,2-Tetrachioroethane 50 --
FORM I VOA
Q
D
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD M-13tr· ' .}'.:'£.i. UD •. ~--)'' UD r•~·
UD
(uL)
uf
(..,'
00059 I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
MP-2C
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix: (soil/water) WATER Lab Sample ID: 9808092-02
lample wt/vol: 25. 00 (g/mL) ML Lab File ID: 809202D2
Level: (low/med) LOW I Moisture: not dee.
GC Column: DB-624 ID: 0. 53 (mm)
Date Sampled: 08/14/98
Date Analyzed: 08/19/98
Dilution Factor: 5o:o
loil Extract Volume: (uL) Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
I
I
I
----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene
108-88-3--------Toluene ------
71-55-6---------1,l,l-Trichloroethane
79-00-5---------1,1,2-Trichloroethane ___ _
79-01-6---------Trichloroethene -------75-01-4---------Vinyl chloride ______ _
1330-20-7-------Xylene(total) --------
FORM I VOA
1000
50
50
50
6.3
50
50
____ (uL)
D
UD
UD
UD
JD
UD
UD
Q
00067 I
I
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-2D
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix:
lample
(soil/water) WATER
wt/vol: 25. 00 (g/mL) ML
Level: (low/med) LOW
I Moisture: not dee.
lfC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808092-03
Lab File ID: 809203D2
Date Sampled: 08/14/98
Date Analyzed: 08/19/98
Dilution Factor: 5.0
loil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone ":JS-8-.-4
71-43-2---------Benzene 5.0
75-27-4---------Bromochloromethane 5.0
75-27-4---------Bromodichloromethane 5.0
75-25-2---------Bromoform 5.0
74-83-9---------Bromomethane 5.0
78-93-3---------2-Butanone 25
75-15-0---------Carbon disulb.de 5.0
56-23-5---------Carbon tetrachloride 5.0
108-90-7--------Chlorobenzene 5.0
75-00-3---------Chloroethane 5.0
67-66-3---------Chloroform 3.0
74-87-3---------Chloromethane 5.0
124-48-1--------Dibromochloromethane 5.0
96-12-8---------1,2-Dibromo-3-chloropropane 5.0
106-93-4--------1,2-Dibromoethane -5.0
95-50-1---------1,2-Dichlorobenzene 5.0
541-73-1--------1,3-Dichlorobenzene 5.0
106-46-7--------1,4-Dichlorobenzene 5.0
75-34-3---------1,1-Dichloroethane 5.0
107-06-2--------1,2-Dichloroethane 5.0
75-35-4---------1,1-Dichloroethene 5.0
156-59-2--------cis-l,2-Dichloroethene 5.0
156-60-5--------trans-l,2-Dichloroethene 5.0
78-87-5---------1,2-Dichloropropane --5.0
10061-01-5------cis-l,3-Dichloropropene 5.0
10061-02-6------trans-l,3-Dichloropropene 5.0
100-41-4--------Ethylbenzene --5.0
591-78-6--------2-Hexanone 25
75-09-2---------Methylene chloride 10
108-10-1--------4-Methyl-2-pentanone 25
100-42-5--------Styrene 5.0
79-34-5---------1,1,2,2-Tetracnloroethane __ 5.0
FORM I VOA
Q
J-B--
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
JD
UD ;;J
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
I FORM 1
00068
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
'ab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
MP-2D
lab Code: NA Batch No. : NA SAS No.: NA . SDG No.: FCX.V0809201
Matrix: (soil/water) WATER
lample wt/vol:
Level: (low/med) I Moisture: not dee.
25. 00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808092-03
Lab File ID: 809203D2
Date Sampled: 08/14/98
Date Analyzed: 08/19/98
Dilution Factor: 5.0
loil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
g
0
B
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene
108-88-3--------Toluene ------
71-55-6---------1,l,l-Trichloroethane
79-00-5---------1,1,2-Trichloroethane ___ _
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride-------
1330-20-7-------Xylene(total) _______ _
FORM I VOA
43 D
5.0 UD
5.0 UD
5.0 UD
2.1 JD
5.0 UD
5.0 UD
Q
00077
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-1B
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix: (soil/water) WATER
lample wt/vol:
Level: (low/med)
'I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808092-04
Lab File ID: 809204D2
Date Sampled: 08/14/98
Date Analyzed: 08/19/98
Dilution Factor: 20.0
loil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
·I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
Q
100 UD
20 UD
20 UD
20 UD
20 UD
20 UD
50 JD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD c' J
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
100 UD
40 UD
100 UD
20 UD
20 UD
I 00078
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
MP-lB
tab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix: (soil/water) WATER
lsample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW
1% Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
lsoil Extract Volume : ____ (uL)
Lab Sample ID: 9808092-04
Lab File ID: 809204D2
Date Sampled: 08/14/98
Date Analyzed: 08/19/98
Dilution Factor: 20.0
Soil Aliquot Volume: ----
ft
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene 250 D
108-88-3--------Toluene 20 UD
71-55-6---------1,1,1-Trichloroethane 20 UD
79-00-5---------1,1,2-Trichloroethane 20 UD
79-01-6---------Trichloroethene 20 UD
75-01-4---------Vinyl chloride 20 UD
1330-20-7-------Xylene(total) 20 UD
FORM I VOA
(uL)
00085
FORM l CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-lC
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix: (soil/water) WATER
tample wt/vol:
Level: (low/med) I Moisture: ?Ot dee.
25. 00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808092-05
Lab File ID: 809205D2
Date Sampled: 08/14/98
Date Analyzed: 08/19/98
Dilution Factor: 10.0 Joil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone 5,; -~
71-43-2---------Benzene 10
75-27-4---------Bromochloromethane 10
75-27-4---------Bromodichloromethane 10
75-25-2---------Bromoform 10
74-83-9---------Bromomethane 10
78-93-3---------2-Butanone 50
75-15-0---------Carbon disulb.de 10
56-23-5---------Carbon tetrachloriae l. 6
108-90-7--------Chlorobenzene 10
75-00-3---------Chloroethane 10
67-66-3---------Chloroform 2.0
74-87-3---------Chloromethane 10
124-48-1--------Dibromochloromethane 10
96-12-8---------1,2-Dibromo-3-chloropropane 10
106-93-4--------1,2-Dibromoethane -10
95-50-1---------1,2-Dichlorobenzene 10
541-73-1--------1,3-Dichlorobenzene 10
166-46-7--------1,4-Dichlorobenzene 10
75-34-3---------1 1-Dichloroethane 10
' ' 107-06-2--------1,2-Dichloroethane 10
75-35-4---------1,l-Dichloroethene 10
156-59-2--------cis-l,2-Dichloroethene 10
156-60-5--------trans-l,2-Dichloroethene 10
78-87-5---------1,2-Dichloropropane --10
10061-01-5------cis-l,3-Dichloropropene 10
10061-02-6------trans-l 3-Dichlorooropene 10 ' . --100-41-4--------Ethylbenzene 10
591-78-6--------2-Hexanone so
7S-09-2---------Methylene chloride 20
108-10-1--------4-Methyl-2-pentanone so
100-42-5--------Styrene 10
79-34-S---------l,l,2,2-Tetrachloroethane 10 --
FORM I VOA
Q
-au--
UD
UD
UD
UD
UD
UD
UD
JD
UD
UD
JD
UD t.J J
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
00086 I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-lC
'ab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
tab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix: (soil/water) WATER
lample wt/vol: 25. 00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm) lloil Extract Volume: ____ (uL)
Lab Sample ID: 9808092-05
Lab File ID: 809205D2
Date Sampled: 08/14/98
Date Analyzed: 08/19/98
Dilution Factor: 10.0
Soil Aliquot Volume: ____ (UL)
D CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I
I
I
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene
108-88-3--

-

-

-

-
-'-Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
170 D
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
00095
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-lD
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Batch No. : NA tab Code: NA
Matrix: (soil/water) WATER
tample wt/vol:
Level: (low/med) I Moisture: not dee.
25. 00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
SAS No.: NA SDG No.: FCX.V0809201
Lab Sample ID: 9808092-06
Lab File ID: 0809206
Date Sampled: 08/14/98
Date Analyzed: 08/19/98
Dilution Factor: 1.0 loil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (uL)
I
0
0
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone 3-·' ~ . l _, ..
71-43-2---------Benzene 1. 0
75-27-4---------Bromochloromethane 1.0
75-27-4---------Bromodichloromethane 1.0
75-25-2---------Bromoform 1.0
74-83-9---------Bromomethane 1.0
78-93-3---------2-Butanone 2.2
75-15-0---------Carbon disulride 1. 0
56-23-5---------Carbon tetrachloride 3.5
108-90-7--------Chlorobenzene 1.0
75-00-3---------Chloroethane 1.0
67-66-3---------Chloroform 1. 5
74-87-3---------Chloromethane 1.0
124-48-1--------Dibromochloromethane 1. 0
96-12-8---------1,2-Dibromo-3-chloropropane 1.0
106-93-4--------1,2-Dibromoethane -1.0
95-50-1---------1,2-Dichlorobenzene 1.0
541-73-1--------1,3-Dichlorobenzene 1.0
106-46-7--------1,4-Dichlorobenzene 1. 0
75-34-3---------1,1-Dichloroethane 1.0
107-06-2--------1,2-Dichloroethane 1.0
75-35-4---------1,1-Dichloroethene 1.0
156-59-2--------cis-l,2-Dichloroethene 1.0
156-60-5--------trans-l,2-Dichloroethene 1.0
78-87-5---------1,2-Dichloropropane --1.0
10061-01-5------cis-l,3-Dichloropropene 1.0
10061-02-6------trans-l,3-Dichloropropene 1.0
100-41-4--------Ethylbenzene --1. 0
591-78-6--------2-Hexanone 5.0
75-09-2---------Methylene chloriae 2.0
108-10-1--------4-Methyl-2-pentanone 5.0
100-42-5--------Stvrene 1.0
79-34-5---------1,i,2,2-Tetrachloroethane 1. 0 --
FORM I VOA
Q . I
fr,/l . ·'{{, ,,/, I ,.,,.A/
I . ._, ·c, (I
u u u u u
J u
u u
u u u u u u
u u
u u u u u u u u u u u u u
00096 I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-lD I Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix: ( soil/water) WATER
lample wt/vol: 25. 00 (g/mL) ML
Level: (low/med) LOW
I Moisture: not dee.
GC Column: DB-624 ID: 0. 53 (mm)
loil Extract Volume: ____ (uL)
Lab Sample ID: 9808092-06
Lab File ID: 0809206
Date Sampled: 08/14/98
Date Analyzed: 08/19/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
I
I
g
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
D
•
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
5.8
0.46 J
1.0 u
1. 0 u
0.65 J
1.0 u
1.0 u
00107 I
I
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-3C
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix:
lample
(soil/water) WATER
wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
,MC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808092-07
Lab File ID: 809207D3
Date Sampled: 08/14/98
Date Analyzed: 08/25/98
Dilution Factor: 5.0
loil Extract Volume: (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
-----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone ;).5
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---0 -----Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulb.cle
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene --78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloricte
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
:;z....+
5.0
5.0
5.0
5.0
5.0
25
5 .. 0
2.0
5.0
5.0
3.1
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
1. 7
5.0
5.0
5.0
5.0
5.0
5.0
25
10
25
5.0
5.0
Q
..:ffi-
UD
UD
UD
UD
UD
UD
UD
JD
UD
UD
JD
UD
UD
UD
UD
UD
UD
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UD
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UD
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UD
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UD
UD
UD
UD
1lSo',·
1-:1-t. -Y'l
;I
,
00108
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-3C
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
tab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix: (soil/water) WATER
lample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW
I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
loil Extract Volume: ____ (uL)
Lab Sample ID: 9808092-07
Lab File ID: 809207D3
Date Sampled: 08/14/98
Date Analyzed: 08/25/98
Dilution Factor: 5.0
Soil Aliquot Volume: ----
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene tJ,fo ·",. -b -----
108-88-3--------Toluene 5.0 UD
71-55-6---------1,1,l-Tricnloroethane 0.78 JD
79-00-5---------1,1,2-Trichloroethane 5.0 UD
79-01-6---------Trichloroethene 6.9 D
75-01-4---------Vinyl chloride 5.0 UD
1330-20-7-------Xylene(total) 5.0 UD
FORM I VOA
(uL)
00129 I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
MP-3D
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix:
lample
(soil/water) WATER
wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW
I Moisture: not dee.
ic Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808092-08
Lab File ID: 809208D3
Date Sampled: 08/14/98
Date Analyzed: 08/25/98
Dilution Factor: 2.5
loil Extract Volume: (uL) -----Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone 71-43-2---------Benzene ___________ _ l:l--~ 2.5
75-27-4---------Bromochloromethane
75-27-4---------Bromodichlorometha_n_e ____ _
75-25-2---------Bromoform 74-83-9---------Bromometh_a_n_e ________ _
78-93-3---------2-Butanone~-~-------
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachlo_r_i_d~e-----
108-90-7--------Chlorobenzene _______ _
75-00-3---------Chloroethane
67-66-3---------Chloroform ---------
74-87-3---------Chloromethane
124-48-1--------Dibromochloro_m_e_t~h_a_n_e ____ _
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenze_n_e ____ _
541-73-1--------1,3-Dichlorobenzene
106-46-7--------l,4-Dichlorobenzene
-----
75-34-3---------1,1-Dichloroethane -----
107-06-2--------l,2-Dichloroethane
75-35-4---------1,l-Dichloroethene ------
156-59-2--------cis-l,2-Dichloroet~h-e_n_e ___ _
156-60-5--------trans~l,2-Dichloroethene __
78-87-5---------1,2-Dichloropropane ____ _
10061-01-5------cis-l,3-Dichloropropene __ _
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone ---------
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentano_n_e ____ _
100-42-5--------Styrene~---~--~----
79-34-5---------1,l,2,2-Tetrachloroethane __
FORM I VOA
2.5
2.5
2.5
2.5
12
2.5
6.7
2.5
2.5
3.2
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.1
2.5
2.5
2.5
2.5
2.5
2.5
12 s 12
2.5
2.5
UD
UD
UD
UD
UD
UD
UD
D
UD
UD
D
UD
UD
UD
UD
UD
UD
UD
UD
UD
JD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
Q
i,I
CJ
-c' J
v
I FORM 1
00130
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I MP-3D
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix: (soil/water) WATER Lab Sample ID: 9808092-08
Lab File ID: 809208D3
Date Sampled: 08/14/98
Date Analyzed: 08/25/98
Dilution Factor: 2.5
lample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW
I Moisture: not dee.
,,;c Column: DB-624 ID: 0.53 (mm)
loil Extract Volume: (uL) ----Soil Aliquot Volume:
I
I
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I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene _____ _ 5J..D :::
108-88-3--------Toluene 2.5
71-55-6---------1,1,1-T_r_i_c~h~lro-r_o_e_t~h.-a_n_e ___ _ 0.88
79-00-5---------1,1,2-Trichloroethane ___ _
79-01-6---------Trichloroethene
2.5
4.8 -------75-01-4---------Vinyl chloride _______ _
1330-20-7-------Xylene(total) _______ _
2.5
2.5
FORM I VOA
____ (uL)
Q
--'))
UD
JD
UD
D
UD
UD
00152 I
I
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-4B
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY tab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0809201
Matrix:
lample
(soil/water) WATER
wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
,iC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808092-09
Lab File ID: 0809209
Date Sampled: 08/14/98
Date Analyzed: 08/25/98
Dilution Factor: 1.0
l,oil Extract Volume: _____ (uL) Soil Aliquot Volume: ----'-(uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone ---5:u -~
71-43-2---------Benzene 1.0
75-27-4---------Bromochloromethane 1.0
75-27-4---------Bromodichloromethane . 1. 0
75-25 0 2---------Bromoform 1.0
74-83-9---------Bromomethane 1.0
78-93-3---------2-Butanone 5.0
75-15-0---------Carbon disulb.de 1.0
56-23-5---------Carbon tetrachlon.de 0.22
108-90-7--------Chlorobenzene 1.0
75-00-3---------Chloroethane 1.0
67-66-3---------Chloroform 1.1
74-87-3---------Chloromethane 1.0
124-48-1--------Dibromochloromethane 1. 0
96-12-8---------1,2-Dibromo-3-chloropropane_ 1.0
106-93-4--------1,2-Dibromoethane 1.0
95-50-1---------1,2-Dichlorobenzene 1. 0
541-73-1--------1,3-Dichlorobenzene 1.0
106-46-7--------1,4-Dichlorobenzene 1.0
75-34-3---------1,1-Dichloroethane 1. 0
107-06-2--------1,2-Dichloroethane 1.4
75-35-4---------1,1-Dichloroethene 0.19
156-59-2--------cis-l,2-Dichloroethene 0.33
156-60-5--------trans~l,2-Dichloroethene __ 1.0
78-87-5---------1,2-Dichloropropane 1. 0
10061-01-5------cis-l,3-Dichloropropene 1. 0
10061-02-6------trans-l,3-Dichloropropene 1.0
100-41-4--------Ethylbenzene --1. 0
591-78-6--------2-Hexanone 5.0
75-09-2---------Methylene chlon.de .;)_, 0 ---. '~
108-10-1--------4-Methyl-2-pentanone 5.0
100-42-5--------Styrene 1. 0
79-34-5---------1,1,2,2-Tetrachloroethane __ l 1.0
FORM I VOA
Q
u " u u u u u u u
J u u
u u u u u u u
u
J
J
u
u u u u u .. u ~
u u u
,-. J
(/
I FORM 1
00153
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
MP-4B
ft Code: NA Batch No. : NA SAS No.: NA SDG No .. : FCX.V0809201
Matrix: (soil/water) WATER Lab Sample ID: 9808092-09
Lab File ID: 0809209
Date Sampled: 08/14/98
Date Analyzed: 08/25/98
Dilution Factor: 1.0
frnple wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW
IMoisture: not dee.
,if Column: DB-624 ID: 0.53 (mm)
~il Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
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I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene
108-88-3--------Toluene ------
71-55-6---------1,l,l-Trichloroethane
79-00-5---------1,1,2-Trichloroethane ___ _
79-01-6---------Trichloroethene -------
75-01-4---------Vinyl chloride ______ _
1330-20-7-------Xylene(total) _______ _
FORM I VOA
I,; ,J ..'.7.,1.-f-E-/)
0.60 J
0.19 J
l.OU
1.1
1.0 U
1.0U
00179
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-4C
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix: (soil/water) WATER
.ample wt/vol: 25. 00 (g/mL) ML
Level: (low/med) .LOW ,. I Moisture: not dee.
GC Column: DB-624 ID: 0. 53 (mm)
Lab Sample ID: 9808092-10
Lab File ID: 809210D3
Date Sampled: 08/14/98
Date Analyzed: 08/25/98
Dilution Factor: 5.0
loil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
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I
I
I
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I
I
I
I
I
CAS NO.
.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1----c----Acetone _;, 5 -6-:--6-
71-43-2---------Benzene 5.0
75-27-4---------Bromochloromethane 5.0
75-27-4---------Bromodichloromethane 5.0
75-25-2---------Bromoform 5.0
74-83-9---------Bromomethane 5.0
78-93-3---------2-Butanone 25
75-15-0---------Carbon disulb.de 5.0
56-23-5---------Carbon tetrachlon.de 3.2
108-90-7--------Chlorobenzene 5.0
75-00-3---------Chloroethane 5.0
67-66-3---------Chloroform 2.6
74-87-3---------Chloromethane 5.0
124-48-1--------Dibromochloromethane 5.0
96-12-8---------1,2-Dibromo-3-chloropropane_ 5.0
106-93-4--------1,2-Dibromoethane 5.0
95-50-1---------1,2-Dichlorobenzene 5.0
541-73-1--------1,3-Dichlorobenzene 5.0
106-46-7--------1,4-Dichlorobenzene 5.0
75-34-3---------1,1-Dichloroethane 5.0
107-06-2--------1,2-Dichloroethane 5.0
75-35-4---------1,1-Dichloroethene 2.8
156-59-2--------cis-l,2-Dichloroethene 5.0
156-60-5--------trans-l,2-Dichloroethene 5.0
78-87-5---------1,2-Dichloropropane --5.0
10061-01-5------cis-l,3-Dichloropropene 5.0
10061-02-6------trans-l,3-Dichloropropene 5.0
100-41-4--------Ethylbenzene --5.0
591-78-6--------2-Hexanone 25
75-09-2---------Methylene chlon.de 10
108-10-1--------4-Methyl-2-pentanone 25
100-42-5--------Styrene 5.0
79-34-5---------1,1,2,2-Tetrachloroethane __ 5.0
FORM I VOA
Q
trB-
UD
UD
UD
UD
UD
UD
UD vs
JD
UD
UD
JD
UD
UD
UD
UD
UD
UD
UD
UD
UD
JD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
FORM 1
0018U
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-4C
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Batch No. : NA lab Code: NA
Matrix: (soil/water)
SAS No.: NA SDG No.: FCX.V0809201
WATER Lab Sample ID: 9808092-10
fample wt/vol: 25.00 (g/mL) ML Lab File ID: 809210D3
Level: (low/med) LOW Date Sampled, 08/14/98
I Moisture: not dee. Date Analyzed: 08/25/98
GC Column: DB-624 ID: 0.53 (mm) Dilution Factor: 5.0
loil Extract Volume: ____ (uL) Soil Aliquot Volume:
I
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I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene /3Ll0 ......... ,..,.. -b
108-88-3--------Toluene 5.0 UD
71-55-6---------1,1,1-Trichloroethane 1.3 JD
79-00-5---------1,1,2-Trichloroethane 5.0 UD
79-01-6---------Trichloroethene 8.9 D
75-01-4---------Vinyl chloride 5.0 UD
1330-20-7-------Xylene(total) 5.0 UD
FORM I VOA
(uL)
00199 I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: ECKENFELDER INC. Contract: EL PASO ENERGY
MP-4D
tb Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix: (soil/water) WATER
tmple wt/vol: 25. 00 . (g/mL) ML
Level: (low/med) LOW
I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808092-11
Lab File ID:
Date Sampled:
0809211D
08/14/98
loil Extract Volume: ____ (uL)
Date Analyzed: 08/18/98
Dilution Factor: 25.0
Soil Aliquot Volume: ____ (uL)
I
I
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I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone /~O
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane
--
10061-01-5--c---cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1 1 2 2-Tetrachloroethane I I I __
FORM I VOA
Q
-r9 ~
25 UD
25 UD
25 UD
25 UD
25 UD
120 UD
25 UD
20 JD
25 UD
25 UD
7.9 JD
25 UD i)J
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
120 UD
50 D
120 UD
25 UD
25 UD
00200
FORM 1 CLIENT SAMPLE NO. I
lab
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-4D
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
.ab ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0809201
'tiatrix: (soil/water) WATER
13ample wt/vol:
Level: (low/med) t Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
lsoil Extract Volume: ____ (uL)
Lab Sample ID: 9808092-11
Lab File ID: 0809211D
Date Sampled: 08/14/98
Date Analyzed: 08/18/98
Dilution Factor: 25.0
Soil Aliquot Volume: ____ (uL)
I
I
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I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene 340 D
108-88-3--------Toluene 25 UD
71-55-6---------1,1,1-Trichloroethane 25 UD
79-00-5---------1,1,2-Trichloroethane 25 UD
79-01-6---------Trichloroethene 8.1 JD
75-01-4---------Vinyl chloride 25 UD
1330-20-7-------Xylene(total) 25 UD
FORM I VOA
I 00210
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
MP-SB
lb Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix: (soil/water) WATER
Jmple wt/vol: 25. 00 (g/mL) ML
Level: (low/med) LOW
I Moisture: not dee.
fif Column: DB-624 ID: 0.53 (mm)
lloil Extract Volume: (uL) ----
Lab Sample ID: 9808092-12
Lab File ID: 0809212D
Date Sampled: 08/14/98
Date Analyzed: 08/19/98
Dilution Factor: 25.0
Soil Aliquot Volume: ----(uL)
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q <---'k"(i. i '1"' (,
1-;ii·-"iY
I
I
I
I
I
I
I
I
67-64-1---------Acetone 71-43-2---------Benzene __________ _
75-27-4---------Bromochloromethane
75-27-4---------Bromodichlorometha_n_e ___ _
75-25-2---------Bromoform 74-83-9---------Bromometh_a_n_e ________ _
78-93-3---------2-Butanone
75-15-0---------Carbon dis_u_l~f~i-a-e ______ _
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene ----
75-00-3---------Chloroethane ________ _
67-66-3---------Chloroform 74-87-3---------Chlorometh~a_n_e _______ _
124-48-1--------Dibromochloromethane ----
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene -----541-73-1--------l,3-Dichlorobenzene ____ _
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane -----
107-06-2--------l,2-Dichloroethane
75-35-4---------1,l-Dichloroethene -----
156-59-2--------cis-l,2-Dichloroet_h_e_n_e __ _
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane_--,-_-_-_-_-
10061-0l-5------cis-l,3-Dichloropropene __ _
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene _c_h_l_o_r_i_a_e _____ _
108-10-1--------4-Methyl-2-pentanone ___ _
100-42-5--------Styrene ____ ~--~---
79-34-5---------1,l,2,2-T~trachloroethane __
FORM I VOA
/~6-_-.-flt 1/
25 UD {,:,ff'
2 5 UD ;""
25 UD
25 UD
25 UD
120 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD ,,J'
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
120 UD
... 5D --:.: ... ~if--' u
120 UD
25 UD
25 UD
00211 I
lab
FORM l CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-5B
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
ltab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0809201
~atrix: (soil/water) WATER
'ample
Level:
wt/vol:
(low/med)
I• Moisture: not dee.
25. 00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0. 53 (mm) '5oil Extract Volume: ____ (uL)
Lab Sample ID: 9808092-12
Lab File ID:
Date Sampled:
0809212D
08/14/98
Date Analyzed: 08/19/98
Dilution Factor: 25.0
Soil Aliquot Volume: ____ (UL)
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene 540 D
I 108-88-3--------Toluene 25 UD
71-55-6---------1,l,l-Trichloroethane 25 UD
79-00-5---------1,1,2-Trichloroethane 25 UD
I 79-01-6---------Trichloroethene 25 UD
75-01-4---------Vinyl chloride 25 UD
1330-20-7-------Xylene(total) 25 UD
I
I
I
I '
11
I
"'
I
I
I
FORM I VOA
I
00217
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-SC
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA
Matrix: (soil/water) WATER
SAS No.: NA SDG No.: FCX.V0809201
Lab Sample ID: 9808092-13
Lab File ID: 0809213D
Date Sampled: 08/14/98
Date Analyzed: 08/24/98
Dilution Factor: 25.0
t ample wt/vol:
Level: (low/med) I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0. 53 (mm)
11,oil Extract Volume: ____ (uL) Soil Aliquot Volume:
I
i:1
I
I·
I
I
I
I
,I
I
••
I
I
CAS NO. COMPOUND
67-64-1---------Acetone
71-43-2---------Benzene
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfiae
56-23-5---------Carbon tetrachloriae
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans~l,2-Dichloroethene __
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chioriae
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1 1 2 2-Tetrachloroethane , , , --
FORM I VOA
120
25
25
25
25
25
120
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
120 so
120
25
25
____ (uL)
Q
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
I 00218
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
MP-SC
lab ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0809201
'atrix: (soil/water) WATER
lample wt/vol:
Level: (low/med) I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm) loil Extract Volume : ____ (uL)
Lab Sample ID: 9808092-13
Lab File ID: 0809213D
Date Sampled: 08/14/98
Date Analyzed: 08/24/98
Dilution Factor: 25.0
Soil Aliquot Volume: ----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene 2 &'''" ~~---)> _, ... .., ..,
108-88-3--------Toluene 25 UD
71-55-6---------1,l,l-Trichloroethane 25 UD
79-00-5---------1,1,2-Trichloroethane 25 UD
79-01-6---------Trichloroethene 17 JD
75-01-4---------Vinyl chloride 25 UD
1330-20-7-------Xylene(total) 25 UD
FORM I VOA
I
(uL)
00230 I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
'ab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
MP-SD
tb Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix: (soil/water) WATER
lample wt/vol: 25. 00 (g/mL) ML
Level: (low/med) LOW
I Moisture: not dee.
GC Column: DB-624 ID: 0. 53 (mm)
Lab Sample ID: 9808092-14
Lab File ID: 0809214D
Date Sampled: 08/14/98
Date Analyzed: 08/24/98
Dilution Factor: 25.0
loil Extract Volume: (uL) -----Soil Aliquot Vo~ume: ____ (uL)
I
,I
I
I
I
I
I
I
.I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6-------~2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
Q
.
120 UD
25 UD
25 UD
25 UD
25 UD
25 UD
120 UD
25 UD UJ'
25 UD
25 UD
25 UD
3.5 JD
25 UD ' 25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
3.9 JD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
120 UD so UD
120 UD
25 UD
25 UD
ii 00231
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
~ab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
MP-SD
'I ab Code : NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix: (soil/water) WATER
lample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
GC Column: DB-624 ID: 0. 53 (mm)
loil Extract Volume: (uL) ----
Lab Sample ID: 9808092-14
Lab File ID: 0809214D
Date Sampled: 08/14/98
Date Analyzed: 08/24/98
Dilution Factor: 25.0
Soil Aliquot Volume: ----
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I'
I
I
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
,),,'Cc, ., -,., ,., =ED --25 UD
25 UD
25 UD
16 JD
25 UD
25 UD
(uL)
I
I
00245
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
TRIP BLANK
#1068-1069
I.ab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix: (soil/water)
lample wt/vol:
ll'evel: (low/med)
I Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
lfC Column: DB-624 ID: 0.53 (mm)
~oil Extract Volume: (uL)
Lab Sample ID: 9808092-15
Lab File ID: 0809215
Date Sampled: 08/14/98
Date Analyzed: 08/18/98
Dilution Factor: 1.0
----Soil Aliquot Volume: ----
I
I
D
H
I
I
I
I
• I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane v
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane
--
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
Q
2.0 JB
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
1.0 u i) .,J
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1. 0 u
1.0 u
1. 0 u
5.0 u
2.1
5.0 u
1.0 u
1.0 u
(uL)
00246
FORM 1 CLIENT SAMPLE NO. I
I
VOLATILE ORGANICS ANALYSIS DATA SHEET TRIP BLANK
#1068-1069
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
Matrix: (soil/water)
'lamp le wt/vol:
llf'evel: (low/med)
I-Moisture: not dee.
fiC Column: DB-624
WATER
25.00 (g/mL) ML
LOW
ID: 0.53 (mm)
&oil Extract Volume: (uL) ----
Lab Sample ID: 9808092-15
Lab File ID: 0809215
Date Sampled: 08/14/98
Date Analyzed: 08/18/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
B
D
I
I
I
E
I
127-18-4--------Tetrachloroethene
108-8~-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
1.0 u
0.12 J
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
00252
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
AS-1
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0809201
Matrix: (soil/water) WATER Lab Sample ID: 9808124-01
Lab File ID: 0812401D
Date Sampled: 08/19/98
Date Analyzed: 08/24/98
Dilu.tion Factor: 25. O
lample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Boil Extract Volume: _____ (uL) Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disu.Lriae
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1 2-Dibromo-3-chlorooropane , . . -
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane -1
FORM I VOA
120
25
25
25
25
25
120
25
25
25
25
4.5
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
120
50
120
25
25
____ (UL)
Q
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
JD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
I
I
I
00253
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
AS-1
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
(
Tab
ab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
.ratrix: (soil/water)
l,ample wt/vol:
,fevel: (low/med)
ll Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
lifC Column: DB-624 ID: 0. 53 (mm)
lsoil Extract Volume: ____ (uL)
Lab Sample ID: 9808124-01
Lab File ID: 0812401D
Date Sampled: 08/19/98
Date Analyzed: 08/24/98
Dilution Factor: 25.0
Soil Aliquot Volume: ----
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
j'3CO ., .., --1> ·---

-
25 UD
25 UD
25 UD
7.3 JD
25 UD
25 UD
(uL)
00268
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
AS-2 Duplicate
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
t b Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0809201
trix: (soil/water) WATER
mample wt/vol:
Level: (low/med)
I Moisture: not dee.
25. 00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808124-02
Lab File ID: 2402DUP
Date Sampled: 08/19/98
Date Analyzed: 08/25/98
Dilution Factor: 10.0
loil Extract Volume : _____ (uL) Soil Aliquot Volume: ----
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone .:,o
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloriae
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
Q
1-6-JB-J
10 UD
10 UD
10 UD
10 UD
10 UD
50 UD
10 UD
15 D
10 UD
10 UD
3.2 JD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
50 UD
24 D J
50 UD
10 UD
10 UD
(uL)
0 FORM 1
00269
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Jb Name: ECKENFELDER INC. Contract: EL PASO ENERGY
AS-2 Duplicate
SAS No.: NA SDG No.: FCX.V0809201 lb Code: NA Batch No.: NA
Matrix: (soil/water) WATER
fmple wt/vol:
Level: (low/med)
I Moisture: not dee.
25. 00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808124-02
Lab File ID: 2402DUP
Date Sampled: 08/19/98
Date Analyzed: 08/25/98
Dilution Factor: 10.0
Jil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (UL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
127-18-4--------Tetrachloroethene
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-88-3--------Toluene ------
71-55-6---------1,l,l-Trichloroethane ----
79-00-5---------1,l,2-Trichloroethane ___ _
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride-------
1330-20-7-------Xylene(total) _______ _
FORM I VOA
100·0
10 UD
10 UD
10 UD
3.0 JD
10 UD
10 UD
Q
00279
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
AS-2
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
gab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
latrix: (soil/water) WATER
oample wt/vol:
Level: (low/med)
I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808124-02
Lab File ID: 812402D2
Date Sampled: 08/19/98
Date Analyzed: 08/25/98
Dilution Factor: 10.0
loil Extract-Volume: _____ (uL) Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6c-------2-Hexanone
75-09-2---------Methylene chloriae
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetracnloroethane __
FORM I VOA
so
10
10
10
10
10
50
10
17
10
10
3.5
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
20
50
10
10
----
Q
UD
UD
UD
UD
UD
UD
UD
UD
D
UD
UD
JD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
(uL)
I 00280
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
AS-2
lll'ab ~ode: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0809201
latrix: (soil/water) WATER
aamnle
'evel:
wt/vol:
(low/med)
I Moisture: not dee.
25.00 (g/mL) ML
LOW
~c Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808124-02
Lab File ID:
Date Sampled:
812402D2
08/19/98
Date Analyzed: 08/25/98
Dilution Factor: 10.0
Soil Aliquot Volume: ----'oil Extract Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene 120 D
108-88-3--------Toluene 10 UD
71-55-6---------1,1,1-Tricnloroethane 10 UD
79-00-5---------1,1,2-Trichloroethane 10 UD
79-01-6---------Trichloroethene 3.2 JD
75-01-4---------Vinyl chloride 10 UD
1330-20-7-------Xylene(total) 10 UD
FORM I VOA
(uL)
00299
FORM l CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-20D 122 FT
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
[
-b ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0809201
trix: (soil/water) WATER
.ample
Level:
wt/vol:
(low/med)
I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808124-05
Lab File ID:
Date Sampled:
0812405
08/17/98
Date Analyzed: 08/24/98
Dilution Factor: 1.0
loil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfiae
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,l-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,l-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetracnloroethane __
FORM I VOA
Q
8.1
1.0 u
1.0 u
2.2
1.0 u
1.0 u
6.3
1.0 u L'.f
1.0 u
l. 0 u
1.0 u
13
1.0 u
0.53 J
l. 0 u
1.0 u
1.0 u
l. 0 u
1.0 u
0.74 J
1.0 u
l. 0 u
0.97 J
l. 0 u
0.31 J
1.0 u
1.0 u
l. 0 u
5.0 u
2.0 u
l. 4 J
1.0 u
1.0 u
00300
FORM 1 CLIENT SAMPLE NO. I
lab
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-20D 122 FT
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
l ab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0809201
atrix: (soil/water) WATER
wample
'level:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW I Moisture: not dee.
GC Column: DB-624 ID: 0. 53 (mm) loil Extract Volume: ____ (uL)
Lab Sample ID: 9808124-05
Lab File ID:
Date Sampled:
0812405
08/17/98
Date Analyzed: 08/24/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
I
I
D
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene 4.9
108-88-3--------Toluene 1.0 u
71-55-6---------1,1,1-Trichloroethane 1.0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 0.69 J
75-01-4---------Vinyl chloride 1.0 u
1330-20-7-------Xylene(total) 1. 0 u
FORM I VOA
I 00351
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: ECKENFELDER INC. Contract: EL PASO ENERGY
TRIP BLANK
#1068-1070
jr-b ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0809201
Ltrix: (soil/water) WATER
[
mple
evel:
wt/vol:
(low/med)
I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808124-07
Lab File ID:
Date Sampled:
0812407
08/19/98
Date Analyzed: 08/24/98
Dilution Factor: 1.0
Soil Aliquot Volume: loil Extract Volume: _____ (uL) ----
B
m
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75~27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-D~bromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
2.3
1.0
1.0
1. 0
1.0
1. 0
5.0
1.0
1.0
1.0
1.0
1.0
1. 0
1.0
1.0
1.0
1.0
1. 0
1. 0
1.0
1.0
1. 0
1.0
1.0
1. 0
1.0
1. 0
1.0
5.0
2.2
5.0
1.0
1. 0
J
u
u
u
u u·
u
u
u
u u
u u
u u u
u u u
u
u
u
u
u
u u u u u
u
u
u
Q
., -• J
(uL)
I 00352
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: ECKENFELDER INC. Contract: EL PASO ENERGY
TRIP BLANK
#1068-1070
l3-b Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0809201
fatrix: (soil/water) WATER
lample
Level:
wt/vol:
(low/med)
I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0. 53 (mm)
loil Extract Volume: ____ (uL)
Lab Sample ID: 9808124-07
Lab File ID:
Date Sampled:
0812407
08/19/98
Date Analyzed: 08/24/98
Dilution Factor: 1.0
Soil Aliquot Volume: ----
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene 1.0 u
108-88-3--------Toluene 0.13 J
71-55-6---------1,1,l-Trichloroethane 1.0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 1.0 u
75-01-4---------Vinyl chloride 1.0 u
1330-20-7-------Xylene(total) 1.0 u
FORM I VOA
(uL)
00359 I
I
FORM 1 CLIENT SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-lC Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0819401
Matrix:
lample
(soil/water) WATER
wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
llf Column: DB-624 ID: O. 53 (mm)
Lab Sample ID: 9808194-01
Lab File ID: 819401D2
Date Sampled: 08/27/98
Date Analyzed: 09/03/98
Dilution Factor: 2.0
loil Extract Volume: (uL) -----Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone /c:--::r ·' • C 71-43-2---------Benzene 2.0 75-27-4---------Bromochloromethane 2.0 75-27-4---------Bromodichloromethane 2.0 75-25-2---------Bromoform 2.0 74-83-9---------Bromomethane 2.0 78-93-3---------2-Butanone 10 75-15-0---------Carbon disulficle 2.0 56-23-5---------Carbon tetrachloricle 2.8 108-90-7--------Chlorobenzene 2.0 75-00-3---------Chloroethane 2.0 67-66-3---------Chloroform 4.5 74-87-3---------Chloromethane 2.0
124-48-1--------Dibromochloromethane 2.0
96-12-8---------1,2-Dibromo-3-chloropropane_ 2.0 106-93-4--------1,2-Dibromoethane 2.0
95-50-1---------1,2-Dichlorobenzene 2.0
541-73-1--------1,3-Dichlorobenzene 2.0
106-46-7--------1,4-Dichlorobenzene 2.0
75-34-3---------1,1-Dichloroethane 2.0
107-06-2--------1,2-Dichloroethane 2.0
75-35-4---------1,1-Dichloroethene 1. 4 156-59-2--------cis-1,2-Dichloroethene 0.84
156-60-5--------trans-1,2-Dichloroethene __ 2.0 78-87-5---------1,2-Dichloropropane 2.0 10061-01-5------cis-1,3-Dichloropropene 2.0 10061-02-6------trans-1,3-Dichloropropene __ 2.0 100-41-4--------Ethylbenzene 2.0 591-78-6--------2-Hexanone 10 75-09-2---------Methylene chloricle ' . .,., -r,, ,, l,, ,Q •..," ---108-10-1--------4-Methyl-2-pentanone 10 100-42-5--------Styrene 2.0 79-34-5---------1 1 2 2-Tetrachloroethane 2.0 ' ' ' --
FORM I VOA
Q
' UD
UD
UD
UD
UD
UD
UD
D
UD
UD
D
UD
UD
UD
UD
UD
UD
UD
UD
UD
JD
JD
UD
UD
UD
UD
UD
UD -,!
~·~
UD
UD
UD
J.J
'I V
00360
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-lC
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
tb Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0819401
Matrix: (soil/water) WATER
.ample wt/vol:
Level: (low/med)
I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
loil Extract Volume : ____ (uL)
Lab Sample ID: 9808194-01
Lab File ID: 819401D2
Date Sampled: 08/27/98
Date Analyzed: 09/03/98
Dilution Factor: 2.0
Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene 530 ~~-)> -
108-88-3--------Toluene 2.0 UD
71-55-6---------1,1,1-Trichloroethane 2.0 UD
79-00-5---------1,1,2-Trichloroethane 2.0 UD
79-01-6---------Trichloroethene 6.0 D
75-01-4---------Vinyl chloride 2.0 UD
1330-20-7-------Xylene(total) 2.0 UD
FORM I VOA
I
I Lab
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
00380
CLIENT SAMPLE NO.
MP-2C
tab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0819401
Matrix: (soil/water) WATER
lample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
fiC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808194-02
Lab File ID: 0819402D
Date Sampled: 08/27/98
Date Analyzed: 09/03/98
Dilution Factor: 50.0
loil Extract Volume: (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
g
u
u
0
u
D
----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-1,2-Dichloroethene
156-60-5--------trans-1,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-1,3-Dichloropropene
10061-02-6------trans-1,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene cnloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1 1 2 2-Tetrachloroethane ' ' ' --
FORM I VOA
250 UD
50 UD
50 UD
50 UD
50 UD
50 UD
250 UD
50 UD
50 UD
50 UD
50 UD
50 UD
50 UD
50 UD
50 UD
50 UD
so UD
50 UD
50 UD
50 UD
so UD
50 UD
50 UD
so UD
50 UD
50 UD
50 UD
50 UD
250 UD
100 UD
250 UD
50 UD
so UD
I 00381
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-2C
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Batch No. : NA tb Code: NA
Matrix: (soil/water)
tmple wt/vol:
SAS No.: NA SDG No.: FCX.V0819401
Level: (low/med)
I Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
loil Extract Volume: ____ (uL)
Lab Sample ID: 9808194-02
Lab File ID: 0819402D
Date Sampled: 08/27/98
Date Analyzed: 09/03/98
Dilution Factor: so.a
Soil Aliquot Volume: ----
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene 280 D
108-88-3--------Toluene 50 UD
71-55-6---------1,1,l-Tricnloroethane 50 UD
79-00-5---------1,1,2-Trichloroethane 50 UD
79-01-6---------Trichloroethene 50 UD
75-01-4---------Vinyl chloride 50 UD
1330-20-7-------Xylene(total) 50 UD
FORM I VOA
(UL)
00385
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-3C
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
fab ~ode: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0819401
"1atrix: (soil/water) WATER
'ample wt/vol:
Level: (low/med) I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808194-03
Lab File ID: 819403D2
Date Sampled: 08/27/98
Date Analyzed: 09/03/98
Dilution Factor: 5.0
loil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2-.--------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloriae
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dithlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4--

-

-

-

-

-

-
-1, 1-Dichlor.oethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
25 UD
5.0 UD
5.0 UD
5.0 UD
5.0 UD
5.0 UD
25 UD
5.0 UD
5.0 UD
5.0 UD
5.0 UD
3.7 JD
5.0 UD ' ;J
5.0 UD
5.0 UD
5.0 UD
5.0 UD
5.0 UD
5.0 UD
5.0 UD
5.0 UD
1.4 JD
5.0 UD
5.0 UD
5.0 UD
5.0 UD
5.0 UD
5.0 UD
25 UD
10 UD
25 UD
5.0 UD
5.0 UD
00386
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-3C
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Batch No. : NA lab Code: NA
Matrix: (soil/water)
'ample wt/vol:
WATER
25. 00 (g/mL) ML
LOW
SAS No.: NA SDG No.: FCX.V0819401
Lab Sample ID: 9808194-03
Lab File ID: 819403D2
Date Sampled: 08/27/98
Date Analyzed: 09/03/98
Dilution Factor: 5.0
Level: (low/med) I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
loil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
0
I
D
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene
108-88-3--------Toluene ------
71-55-6---------1,l,l-Trichloroethane
79-00-5---------1,1,2-Trichloroethane ___ _
79-01-6---------Trichloroethene -------75-01-4---------Vinyl chloride _______ _
1330-20-7-------Xylene(total) _______ _
FORM I VOA
Q
~ --]) . -..., .....,._.
5.0 UD
5.0 UD
5.0 UD
5.8 D
5.0 UD
5.0 UD
I FORM 1
00402
CLIENT SAMPLE NO.
I
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-4C
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0819401
Matrix: (soil/water)
lample wt/vol:
J,evel: (low/med)
I-Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
_,c Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808194-04
Lab File ID: 0819404D
Date Sampled: 08/27/98
Date Analyzed: 09/03/98
Dilution Factor: 100.0
-=,oil Extract Volume: (uL) ----Soil Aliquot Volume:
I
I
I
I
g
n
u
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane
--
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
500
100
100
100
100
100
500
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
500
200
500
100
100
____ (uL)
Q
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
I FORM 1
00403
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-4C I -Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0819401
Matrix: (soil/water) WATER
··ample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW
I Moisture:-not dee.
rjC Column: DB-624 ID: 0.53 (mm)
.loil Extract Volume: (uL) ----
Lab Sample ID: 9808194-04
Lab File ID: 0819404D
Date Sampled: 08/27/98
Date Analyzed: 09/03/98
Dilution Factor: 100.0
Soil Aliquot Volume: ___ ,_(UL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
D
0
I
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
1200 D
100· UD
100 UD
100 UD
100 UD
100 UD
100 UD
I
lab
00407
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-SC
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0819401
atrix: (soil/water) WATER
lample wt/vol:
Level: (low/med)
I .Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808194-05
Lab File ID: 0819405D
Date Sampled: 08/27/98
Date Analyzed: 09/03/98
Dilution Factor: 250.0
loil Extract Volume : ____ (uL) Soil Aliquot Volume: ____ (uL)
I
0
D
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
67-64-1---------Acetone
71-43-2---------Benzene
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disuliioe
56-23-5---------Carbon tetrachlorioe
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l 2-Dichloroethene , --
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chlorioe
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA,
1200 UD
250 UD
250 UD
250 UD
250 UD
250 UD
1200 UD
250 UD
250 UD
250 UD
250 UD
250 UD
250 UD i .. FJ
250 UD
250 UD
250 UD
250 UD
250 UD
250 UD
250 UD
250 UD
250 UD
250 UD
250 UD
250 UD
250 UD
250 UD
250 UD
1200 UD
500 UD
1200 UD
250 UD
250 UD
00408
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-SC
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
[
b ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0819401
trix: (soil/water) WATER
tmple wt/vol:
Level: (low/med)
I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID:.0.53 (mm)
· loil Extract Volume: ____ (uL)
Lab Sample ID: 9808194-05
Lab File ID: 0819405D
Date Sampled: 08/27/98
Date Analyzed: 09/03/98
Dilution Factor: 250.0
Soil Aliquot Volume: ----
I
I
I
I
0
D
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,1,l-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
3100 D
250 UD
250 UD
250 UD
250 UD
250 UD
250 UD
(uL)
00413
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
AS-2
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
fiab ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0819401
llf.iatrix: (soil/water) WATER
fample wt/vol:
Level: (low/med)
IJ Moisture: not dee.
25. 00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808194-06
Lab File ID: 0819406
Date Sampled: 08/27/98
Date Analyzed: 09/04/98
Dilution Factor: 1.0
lloil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
g
H
D
m
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone s
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
. ~
~-~ 1.0
1.0
1.0
1. 0
1.0
5.0
1.0
4.5
1.0
1.0
1.8
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.12
1.0
1.0
1.0
1.0
1.0
1.0
5.0
75-09-2---------Methylene chloride ~,O "'.:-
108-10-1--------4-Methyl-2-pentanone 5.0
100-42-5--------Styrene 1.0
79-34-5---------1,1,2,2-Tetrachloroethane __ 1.0
FORM I VOA
Q
V u
u
u u
u u
u
u u
u u u u u
u u
u
u
J u u
u
u u u u -V V
u u
u
'
\
-k'lu ..
,-1-t-'fff
v
jJ
u
00414
FORM l CLIENT SAMPLE NO. I
lab
VOLATILE ORGANICS ANALYSIS DATA SHEET
AS-2
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
1ab ~ode: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0819401
'atrix: (soil/water) WATER
'ample wt/vol:
Level: (low/med) I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm) loil Extract Volume: ____ (uL)
Lab Sample ID: 9808194-06
Lab File ID: 0819406
Date Sampled: 08/27/98
Date Analyzed: 09/04/98
Dilution Factor: 1.0
Soil Aliquot Volume:
g
0
D
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,l,l-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
19
1.0 u
1.0 u
1.0 u
l. 2
l. 0 u
1.0 u
I
lab
00428
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
AS-1
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lf'ab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0819401
~atrix: (soil/water) WATER Lab Sample ID: 9808194-07
tample
Level:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
Lab File ID:
Date Sampled:
819407D2
08/27/98
[t Moisture: not dee. Date Analyzed: 09/04/98
Dilution Factor: 2.0
Soil Aliquot Volume:
GC Column: DB-624 ID: 0.53 (mm)
llsoil Extract Volume: ____ (uL)
D
D
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I
I
I
I
I
I
I
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1~-------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene --78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
·o .---I ~--'
2.0
2.0
2.0
2.0
2.0
10
0.22
2.0
2.0
2. 0.
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
10 4-o~ · .~
10
2.0
2.0
~~ V
UD
UD
UD
UD
UD
UD
JD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
,HJ
UD
UD
UD
J
u
00429
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
AS-1
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
tab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0819401
Matrix: (soil/water)
ll5ample wt/vol:
Level: (low/med)
1% Moisture: not dee.
WATER
25. 00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
!soil Extract Volume: ____ (uL)
Lab Sample ID: 9808194-07
Lab File ID: 819407D2
Date Sampled: 08/27/98
Date Analyzed: 09/04/98
Dilution Factor: 2.0
Soil Aliquot Volume: ----'--(UL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127~18-4--------Tetrachloroethene 40 D
108-88-3-~------Toluene 2.0 UD
71-55-6---------1,1,1-Trichloroethane 2.0 UD
79-00-5---------1,1,2-Trichloroethane 2.0 UD
79-01-6---------Trichloroethene 2.0 UD
75-01-4---------Vinyl chloride 2.0 UD
1330-20-7-------Xylene(total) 2.0 UD
FORM I VOA
00439
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-3B
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Batch No. : NA lab Code: NA
Matrix: ( soil/water)
.ample wt/vol:
SAS No.: NA SDG No.: FCX.V0819401
Level: (low/med)
I Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808194-08
Lab File ID: 0819408D
Date Sampled: 08/28/98
Date Ahalyzed: 09/04/98
Dilution Factor: 50.0
Soil Aliquot Volume: loil Extract Volume : ____ (uL) ----
D
0
I
•
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfl.de
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-D~bromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5------~--l,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1~-------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachioroethane __
FORM I VOA
Q
250 UD so UD so UD so UD so UD so UD
250 UD so UD so UD so UD so UD so UD so UD uJ so UD so UD uT
so UD so UD so UD so UD so UD so UD so UD so UD so UD so UD so UD so UD so UD
250 UD
100 UD
250 UD so UD so UD
(uL)
I 00440
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-3B
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
fiab ~ode: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0819401
llatrix: (soil/water) WATER
liample
'!evel:
wt/vol:
(low/med) I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0. 53 (mm)
11,oil Extract Volume: ____ (uL)
Lab Sample ID: 9808194-08
Lab File ID:
Date Sampled:
0819408D
08/28/98
Date Analyzed, 09/04/98
Dilution Factor: 50.0
Soil Aliquot Volume: ----
D
D
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
820 D
50 UD
50 UD
50 UD
50 UD
50 UD
50 UD
(uL)
00447
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-3D
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
iLab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0819401
Matrix: (soil/water) WATER
tample wt/vol:
Level: (low/med)
1% Moisture: not dee ..
25. 00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808194-09
Lab File ID: 0819409D
Date Sampled: 08/28/98
Date Analyzed: 09/04/98
Dilution Factor: 25.0
lsoil Extract Volume: ____ (uL) Soil Aliquot Volume: ----
D
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane .
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-D~bromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene --78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride .so
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
Q
120 UD
25 UD
25 UD
25 UD
25 UD
25 UD
120 UD
25 UD
8.3 JD
25 UD
25 UD
3.1 JD
25 UD t.iJ
25 UD
25 UD JJ
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
120 UD
-5-;-6 JB i)
120 UD
25 UD
25 UD
(uL)
00448 I
lab
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-3D
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
f'ab ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0819401
~atrix: (soil/water) WATER
rample
Level:
wt/vol:
(low/med) t Moisture: not dee.
25. 00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
'3oil Extract Volume: ____ (uL)
Lab Sample ID: 9808194-09
Lab File ID:
Date Sampled:
0819409D
08/28/98
Date Analyzed: 09/04/98
Dilution Factor: 25.0
Soil Aliquot Volume: ____ (uL)
I
g
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
D
I
I
I
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
290 D
25 UD
25 UD
25 UD
3.1 JD
25 UD
25 UD
00457 I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-2B
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lilab ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0819401
latrix: (soil/water) WATER
iample
~evel:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808194-10
Lab File ID:
Date Sampled:
0819410D
08/28/98
loil Extract Volume: ____ (uL)
Date Analyzed: 09/04/98
Dilution Factor: 25.0
Soil Aliquot Volume: ____ (uL)
D
D
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12"8---------1,2-Dibromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene --78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
Q
120 UD
25 UD
25 UD
25 UD
25 UD
25 UD
120 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD OJ
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
120 UD
50 UD
120 UD
25 UD
25 UD
ii
1,
1 jl 1,
l ii
'1
I
I
I
D
u
I
I
I
I
00458
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET CLIENT SAMPLE NO.
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY MP-2B
Lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0819401
Matrix: (soil/water) WATER Lab Sample ID: 9808194-10
Sample wt/vol: Lab File ID: 0819410D
Level: (low/med)
% Moisture: not dee.
GC Column: DB-624
25.00 (g/mL) ML
LOW
ID: 0. 53 (mm)
Date Sampled: 08/28/98
Date Analyzed: 09/04/98
Dilution Factor: 25.0
Soil Extract Volume: (uL) ----Soil Aliquot Volume: ____ (uL)
CAS NO. COMPOUND
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
------
71-55-6---------1,1,1-T~rci~c~h~r~o~r~o~e~t~h"a~n~e-=----
79-00-5---------l,l,2-Trichloroethane
79-01-6---------Trichloroethene ----
75-01-4---------Vinyl chloride ______ _
1330-20-7-------Xylene(total) _______ _
FORM I VOA
330 D
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
Q
00463 I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
TRIP BLANK
#1085&1086
fab ~ode: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0819401
"1atrix: (soil/water) WATER Lab Sample ID: 9808194-11
'ample
Level:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
Lab File ID:
Date Sampled:
0819411
08/27/98
I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Date Analyzed: 09/03/98
Dilution Factor: 1.0
Roil Extract Volume : ____ (uL) Soil Aliquot Volume:
n
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------i-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-D~bromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-1,2-Dichloroethene
156-60-5--------trans-1,2-Dichloroethene --78-87-5---------1,2-Dichloropropane
10061-01-5------cis-1,3-Dichloropropene
10061-02-6------trans-1,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
3.4
1. 0
1.0
1.0
1.0
1. 0
5.0
1.0
1.0
1. 0
1.0
1.0
1.0
1.0
1. 0
1. 0
1.0
1.0
1.0
1.0
1.0
1. 0
1.0
1.0
1. 0
1.0
1.0
1.0
5.0
1.0
5.0
1.0
1.0
____ (uL)
Q
J u u u u u u u u u u u u u u u u u u u u u u u u u u u u
J u u u
00464
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
TRIP BLANK
#1085&1086
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
1ab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0819401
latrix: (soil/water) WATER
.ample wt/vol:
Level: (low/med)
I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
loil Extract Volume : ____ (uL)
Lab Sample ID: 9808194-11
Lab File ID: 0819411
Date Sampled: 08/27/98
Date Analyzed: 09/03/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
D
m
I
I
I
I
I
I
I
I
I
I
I
. CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene 1.0 u
108-88-3--------Toluene 1.0 u
71-55-6---------1,1,l-Trichloroethane 1.0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 1.0 u
75-01-4---------Vinyl chloride 1.0 u
1330-20-7-------Xylene(total) 1.0 u
FORM I VOA
00469 I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-1B
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
ai,ab ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0819401
'atrix: (soil/water) WATER
1sample
Level:
wt/vol:
(low/med)
1% Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808194-12
Lab File ID: 0819412D
Date Sampled: ·. 08/28/98
Date Analyzed: 09/04/98
Dilution Factor: 25.0
Osoil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ .(UL)
u
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---~-----Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-50--------Carbon tetrachloride-
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12~8---------1,2-D~bromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
Q
120 UD
25 UD
25 UD
25 UD
25 UD
25 UD
120 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD JJ
·_25 UD
25 UD u.f 25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
120 UD
50 UD
120 UD
25 UD
25 UD
00470
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MP-lB
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Batch No. : NA lab Code: NA
Matrix: (soil/water)
SAS No.: NA SDG No.: FCX.V0819401
WATER
lample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
lloil Extract Volume: (uL) ----
Lab Sample ID: 9808194-12
Lab File ID: 0819412D
Date Sampled: 08/28/98
Date Analyzed: 09/04/98
Dilution Factor: 25.0
Soil Aliquot Volume: ____ (uL)
0
D
m
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
Q lf!;l~
530 D
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
00475
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
STORAGE BLANK
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
[
b ~ode: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0819401
atrix: (soil/water) WATER
lample
Level:
wt/vol:
(low/med)
I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9808194-13
Lab File ID:
Date Sampled:
STORBLK
08/29/98
Date Analyzed: 08/25/98
Dilution Factor: 1.0
loil Extract Volume : ____ (uL) Soil Aliquot Volume: ____ (uL)
I
D
m
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3-J-------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2 -·--

-

-

-

-

-
-Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
Q
1. 8 J
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
.1.0 u uJ
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
5.0 u
1. 2 J
5.0 u
1. 0 u
1.0 u
00476
FORM 1 CLIENT SAMPLE NO. JI VOLATILE ORGANICS ANALYSIS DATA SHEET
STORAGE BLANK ] ILab Name: ECKENFELDER INC. Contract: EL PASO ENERGY l Lab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0819401
IMatrix: (soil/water) WATER I Sample wt/vol: 25.00 (g/mL) ML
ILevel: (low/med) LOW ! 1%-Moisture: not dee.
, GC Column: DB-624 ID: 0.53 (mm)
I ' ISoil Extract Volume: ____ (uL)
Lab Sample ID: 9808194-13
Lab File ID:
Date Sampled:
STORBLK
08/29/98
Date Analyzed: 08/25/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
I
I
I
n
D
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5--~------1,l,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
1.0 u
1.0 U.
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u