NCD095458527_19990301_FCX Inc. (Statesville)_FRBCERCLA RI_Pre-Design Investigative Report for OU-3-OCR

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PRE-DESIGN INVEST/GA TION REPORT
FOR OPERABLE UNIT THREE (OU3)
FCX-STATESVILLE SUPERFUNO SITE,
STATESVILLE, NORTH CAROLINA
VOLUME 3
prepared for
El Paso Energy Corporation
1001 Louisiana Street
Houston. TX 77002
March 1999
27-<,m 13.008
RECEIVED
MAR 22 7999
SUPERFUND SECTION
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APPENDIX F-5
DATA VALIDATION REPORTS DATED
MARCH 1, 1999
\ \ TN'\SYS\DAT A \PROJ\.03 13.08 \PDI-CVR.DOC
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DATA VALIDATION REPORT
FCX Statesville
(FCX299A)
Prepared By
Environmental Data Services, Ltd.
For
Eckenfelder, Inc.
March 1, 1999
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I DAT A ASSESSMENT NARRATIVES
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DATA ASSESSMENT NARRATIVE FOR VOLATILES
SITE: FCX Statesville
LABORATORY: Eckenfelder, Inc.
SAMPLE DELIVERY GROUP: FCX299A
This sample delivery group consists of the following water samples:
W-20I W-31I W-12I W-31S
W-AB Trin Blank #1204 Holdinn Blank 12-17-98 AA121798
W-5s W-Bi . W-26i W-18s
W-9s W-20D W-16s W-16I
Holdinn Blank 12-18-98 W-28i W-AD W-17s
Trio Blank #1209 Holdinn Blank 12-21-98 W-30I W-10I
W-29i W-AC W-22s W-22I
W-1s W-205 Trio Blank #1202 Holdina Blank 12-22-98
W-AA
W-24s
W-19s
Trin Blank #1086
W-32I
W-5I
W-AE
W-18I
Samples described above were analyzed via USEPA Low Level CLP SOW OLC01.0 to determine the
concentration of volatiles in water.
USEPA Contract Laboratory Program National Functional Guidelines for Organic Data Review (February
1994) have been considered during the validation of this data and in determining its usability.
All data are valid and acceptable except those analytes which have been qualified as described in the
attached glossary. All data qualification related to this group of samples is detailed on the attached
sheets.
Major Data Quality Issues
Calibration -All initial and continuing calibrations had various target compounds with extremely low
response factors i.e., less than 0.05. Associated not detected sample results for the effected
compounds have been fiagged "R" unusable.
Minor Data Quality Issues
Blank Contamination -Various target analytes were present in method, field and trip blanks associated
with samples in this delivery group. Effected compound results have been qualified per USEPA
guidelines.
Continuing Calibration -Several continuing calibrations had observed percent difference values for
various target analytes that failed to meet validation criteria. All sample analyses associated with
the non-compliant continuing calibrations have been qualified as estimated.
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Surrogate Standard Recoveries -Several sample analyses exhibited less than acceptable surrogate
standard recoveries. Effected sample results have been flagged as estimated where appropriate.
Internal Standard Recovery -One sample exhibited less than acceptable area counts for all internal
standards. All sample results not previously qualified as unusable for the effected sample have
been flagged as estimated.
Holding Time -One sample was verified to have a pH of greater than 2. Because the sample analysis
was not performed within seven days of collection, all aromatic hydrocarbon results were qualified
as estimated.
Linear Range Exceedence -One sample result was reported based on an instrument response above
the highest calibration standard. The effected sample results was flagged" J" estimated.
Two facts should be noted by all data users. First, the "R" flag means that the associated value is
unusable due to significant QC problems, the data is invalid and provides no information as to whether
the compound is present or not. "R" values should not appear on any data tables even as a last resort.
Lastly, strict QC serves to increase confidence in data but any value potentially contains error.
Date:
\ . Environmental Scientist/Director
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HOLDING TIME
The amount of an analyte can change with time due to chemical instability, degradation, volatilization, etc.
If the specified holding time is exceeded the data may not be valid.
The analyses performed on samples in this sample delivery group were all done within established
holding times with the following exception.
Sample W-10i was found to have a pH of greater than 2. The sample was not analyzed within seven days
of collection. Therefore, all aromatic hydrocarbon results for sample W-10i.
BLANK CONTAMINATION
Quality assurance blanks, method, trip, field, or rinse blanks are prepared to identify any contamination
which may have been introduced into the samples during preparation or field activity. Method blanks
measure lab contamination. Trip blanks measure cross contamination during shipment. Field and rinse
blanks measure cross contamination during field operations.
Method Blank Contamination
Method blanks were analyzed at the proper frequency. Upon examination, the method blanks did not
contain any target analy1e at or above reportable concentration levels with the following exceptions.
The method blank performed on 12/22198 (VBLK 1222) was found to contain positive results for the
following target analy1es:
acetone
methylene chloride
toluene
2 ppb
0.09 ppb
0.04 ppb
The following samples were analyzed in association with method blank VBLK1222. Effected results for
the samples listed were qualified based on validation guidelines as appropriate.
W-31i W-31s W-AA W-24s W-81
W-161 W-1s W-281 W-9s
The method blank performed on 12/23/98 (VBLK 1223) was found to contain positive results for
methylene chloride (0.08 ppb) and toluene (0.03 ppb). Trip blank, holding blank and field blank samples
were associated with method blank VBLK1223. According to validation guidelines blank sample results
are not qualified when associated with other non-compliant blanks. Therefore, no data qualification was
applied.
The method blank performed on 12/26/98 (VBLK 1226) was found to contain positive results for
chloromethane (0.08 ppb) and methylene chloride (0.2 ppb).
The following samples were analyzed in association with method blank (VBLK 1226). Effected sample
results for the samples listed were qualified based on validation guidelines as appropriate.
! W-201 I W-19s ! W-181 I W-161 I W-165 I AA121798
The method blank performed on 12-27-98 (VBLK1227) was found to contain ethyl benzene (0.05 ppb)
and xylene total (0.1 ppb). None of the sample analyses associated with VBLK 1227 required
qualification based on method blank contamination.
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The method blank perfonned on 12/31/98 (VBLK 1231) was found to contain positive results for benzene
(0.06 ppb) and 1, 1-dichloroethene (0.1 ppb). The following samples were analyzed in association with
method blank VBLK 1231. Effected results for the samples listed have been qualified as appropriate.
J W-32I 1 W-17s I W-10I I W-22s i W-20s
The method blank perfonned on 1/1/99 (VBLK 0101) was found to contain a positive result for methylene
chloride (0.18 ppb). The following samples were analyzed in association with method blank VBLK 0101.
Methylene chloride results for the samples listed have been qualified as appropriate.
J W-22I I W-AC I W-29I I W-5I
Field Blank/Trip Blank/Holding Blank Contamination
Field, trip and holding blank sets were collected throughout the field sampling event.
Upon evaluation associated trip, field and holding blank samples were found to be free of target 3nalytes
with the following exceptions:
Blanks Chloromethane Toluene Methylene Chloride
WAS <Eauioment Blank) 12-18-98 0.1 0.07 0.9
Trio Blank #1204 12-16-98 0.07 0.06 0.7
Holdina Blank 12-17-98 --0.1
Samples associated with the control blanks listed above were carefully evaluated and have been
appropriately qualified based on the blank contamination observed.
Blanks Chloromethane Toluene Methylene Tetrachloro-
Chloride ethene
WAD (Eauiomenl Blank) 12-18-98 0.2 0.1 0.8 ----
Trio Blank#108612-17-98 -0.05 0.7 0.2
Holdina Blank 12-18-98 --0.1 -
Samples associated with the control blanks listed above were carefully evaluated and have been
appropriately qualified based on the blank contamination observed.
Blanks Chloromethane Toluene Methylene 1, 1-dichloro-
Chloride ethene
WAE rEauiomenl Blank) 12-19-98 0.2 --0.1
Trip Blank #1209 12-18-98 -0.04 1 -
Holdina Blank 1 2-21-98 --0.1 -
Samples associated with the control blanks listed above were carefully evaluated and have been
appropriately qualified based on the blank contamination observed.
Blanks Benzene 1, 1-dichloroethene Methvlene Chloride
Trio Blank #1204 12-16-98 0.06 0.1 0.5
Holdina Blank 12-17-98 ---
Samples associated with the control blanks listed above were carefully evaluated and have been
appropriately qualified based on the blank contamination observed.
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MASS SPECTROMETER TUNING
Tuning and performance criteria are established to ensure adequate mass resolution, proper identification
of compounds, and to some degree, sufficient instrument sensitivity. These criteria are not sample
specific. Instrument performance is determined using standard materials. Therefore, these criteria should
be met in all circumstances.
The tuning standard for volatiles is bromofluorobenzene (BFB).
All tunes associated with this SDG were fully compliant.
CALIBRATION
Satisfactory instrument calibration is established-to ensure that the instrument is capable of producing
acceptable quantitative results. The initial calibration curve demonstrates that the instrument is capable of
giving acceptable performance at the beginning of an analytical sequence. The continuing calibration
verifies that the instrument is giving satisfactory daily performance.
Response Factor I
The response factor measures the instruments responses to specific chemical compounds. The response
factors for the VOA Target Compound List must be greater than or equal to 0.05 in both the initial and
continuing calibrations. A value less than 0.05 indicates serious detection and quantitation problems.
RRF values in all initial and continuing calibrations were greater than 0.05 with the following exceptions.
The initial calibration performed on 12/22/98 as well as all continuing calibrations that followed had
extremely low i.e., (less than 0.05) response factors observed for acetone and 1,2-dibromo-3-chloro-
propane.
The following sample analyses were associated with the calibrations described above:
W31i W31s W-AA W-24s
W8i W-161 W-1s W-28i
W30i w-9s Trio Blank #1 204 W-AB
Ho!dina Blank 121798 W-121 Trlo Blank #1086 Holdin □ Blank 121898
W-20D W-261 W-1Bs
All non-detect acetone and 1 ,2-dibromo-3-chloromethane results for the samples listed above have been
flagged "R" unusable. Positive results for the effected compounds were qualified "J" estimated.
The initial calibration performed on 12/26/98 had extremely low i.e., (less than 0.05) response factors
observed for the following compounds:
acetone
2-butanone
1,2-dibromo-3-chloropropane
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The following sample analyses were associated with the calibration described above:
W-201 AA121798 Trio Blank 1209 W-19s W-AD
W-22I W-18I W-AC W-16I W-5s
W-29I W-9s Holdinn Blank 122198 W-5I Holdinn Blank 122298
Trr Blank 1202 W-32I W-17s W-10i W-22s
WAE W-205
All non-detect acetone, 2-butanone and 1,2-dibromo-3-chloropropane results for the samples listed above
have been fiagged "R" unusable. Positive results for the effected compounds have been fiagged "J"
estimated.
Additionally the continuing calibrations performed on 12/26/98 and 12/27 /98 had extremely low response
factors observed for bromoform. The following samples were associated with the calibrations described
above and since all bromoform results were not detected, have been fiagged "R" unusable.
W-AD W-19s W-5s Holdin Blank 122198 Tri Blank 1209
W-20I W-18I W-16I W-16S AA121798
Percent Relative Standard Deviation (RSD) and Percent Deviation (¾D)
Percent RSD is calculated from the inttial calibration and is used to indicate stabiltty of a specific
compound over the calibration range. %D compares the response factor of the continuing calibration with
the mean response factor of the initial calibration. Therefore %D is a measure of the instruments daily
performance.
The following QC criteria has been applied for this project:
% RSD of initial calibration must be <30.0 %
% D for continuing calibrations must be <25.0%
A value outside these limits indicates potential detection and quantitation errors. According to the USEPA
CLP National Functional Guidelines for Organic Data Review (2/94), all positive and non-detect results
are flagged as estimated.
The initial and continuing calibrations associated with this sample delivery group met all validation criteria
with the following exceptions.
The continuing calibration performed on 12/23/98 had an observed percent difference value for 1, 1,2,2-
tetrachloroethane (28.8%) that fell outside validation acceptance criteria. The following sample analyses
were associated with the calibration described above:
II Trip Blank #1204 I Holding Blank 121798 I W-AB
1, 1,2,2-tetrachloroethane results for the samples listed above have been fiagged "UJ" estimated.
The continuing calibration performed on 12/25/98 had observed percent difference values for carbon
tetrachloride (29.3) and tetrachloroethene (27.3%) that fell outside validation acceptance criteria. The
following sample analyses were associated with the calibration described above.
W-12I Tri Blank #1086 Holdin Blank 121898 W-20D W-26i
Effected compound results for the samples listed above have been nagged as estimated" J"rUJ".
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The continuing calibration perfonnned on 12/27 /98 had observed percent difference values for the
following compounds that fell outside validation acceptance criteria:
bromomethane
1,2-dibromo-3-chloropropane
1, 1-dichloroethane
51.0%
32.4%
30.7%
The following sample analyses were associated with the calibration described above:
W-AD W-5s Holdin Blank 122198 Tri Blank 1209
Effected compound results for the samples listed above when not previously rejected have been nagged
as estimated "J"rUJ".
The continuing calibration perfonnned on 1/1/99 had observed percent difference values for the following
compounds that fell outside validation guidelines:
acetone
bromomethane
bromochloromethane
methylene chloride
tetrachloroethene
chlorofonnn
chloromethane
1, 1-dichloroethane
cis-1 ,2-dichloroethene
40.7%
67.3%
42.8%
31.2%
33.8%
30.5%
26.4%
29.9%
31.4%
The following sample analyses are associated with the calibration described above:
I W-20SDL I W-22I I W-1SDL I W-30IDL I W-AC I W-29I I W-5I
Effected compound results for the samples listed above when not previously rejected have been flagged
as estimated "J"/"UJ".
The continuing calibration perfonnned on 12/31 /98 had observed percent difference values for the
following compounds that fell outside validation guidelines:
carbon tetrachloride
bromochloromethane
bromomethane
2-butanone
2-hexanone
methylene chloride
4-methyl 2-pentanone
cis-1,2-dichloroethene
31.9%
34.0%
56.3%
26.1%
66.7%
31.0%
41.4%
26.0%
The following sample analyses are associated with the calibration described above:
Holdin Blank 122298 Tri Blank #1202 W-32I W-17s
W-22s W-AE W-20s
Effected compound results for the samples listed above when not previously rejected have been flagged
as estimated "J"rUJ".
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INTERNAL STANDARDS PERFORMANCE
Internal standard performance criteria is meant to ensure that the GC/MS sensitivity and response are
stable during every experimental run.
The internal standard area count must not vary by more than a factor of two from the associated
continuing calibration standard. The retention time of the internal standard must not vary by more than +/-
30 seconds from the associated continuing calibration standard. If the area count is outside the (-50% -
100%) range of the associated standard, all positive results for compounds quantitated using that
standard are qualified as estimated, and non detects as UJ, but only if area is< 50%.
Internal standard recoveries observed in all samples and method blanks were within acceptable limits
with one exception.
Trip blank #1086 had observed standard areas for all internal standards below the lowest allowable level.
All compound results not previously reject for Trip Blank #1086 have been nagged as estimated "J"rUJ".
SURROGATES
All samples and blanks are spiked with surrogate compounds prior to sample preparation and analyses to
evaluate overall laboratory performance and efficiency of the analytical technique.
All samples and method blanks evaluated in this report had observed surrogate recoveries within the
established limits with the following exceptions:
Trip blank #1086 had an observed surrogate standard recovery above the highest allowable limit. All
sample results for Trip Blank #1086 were previously nagged as estimated due to poor internal standard or
rejected based on calibration criteria. No further qualification of the sample data was necessary.
Sample analyses W-24SDL and W-19SDL each had one observed surrogate standard recovery fall below
the lowest allowable level. The tetrachloroethene results reported from these analyses have been
nagged "J" estimated.
Sample W-5S had one surrogate standard recovery observed below the lowest allowable level. All W-5s
sample results not previously nagged "R" unusable have been qualified as estimated.
COMPOUND IDENTIFICATION
Volatile
TCL compounds are identified on the GC/MS by using the analyte's relative retention time (RRT) and ion
spectra. For the results to be a positive hit, the sample peak must be within:!: 0.06 RRT units of the
standard compound, and have an ion spectra which has a ratio of the primary and secondary ion
intensities within 20% of that in the standard compound. No analytes were qualified for compound
identification.
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MATRIX SPIKE/MATRIX SPIKE DUPLICATE
The matrix spike and matrix spike duplicate are generated to determine the precision and accuracy of the
analytical procedure in a given matrix. This information may be used to qualify data.
No sample from this delivery group was analyzed as matrix spike/matrix spike duplicate pair. Therefore,
no evaluation of matrix specific precision and accuracy indicators could be performed.
Laboratory control samples were processed at a frequency of one per twelve hour analysis period. LCS
recoveries were well within acceptance limits in every case.
OTHER QC DATA OUT OF SPECIFICATION
The tetrachloroethene result for sample W-8I was reported based on an instrument response outside the
linear range. The effected sample result was flagged "J" estimated.
FIELD DUPLICATE
Samples W-AA and W-31s) and ry,,J-AC and W-29i) comprise the field duplicate pairs associated with
samples in this delivery group. Field precision exhibited was extremely good. The largest percent
difference observed for positively identified target analytes between either pair was less than 29%. Field
precision was demonstrated to be well within acceptable tolerances.
SYSTEM PERFORMANCE AND OVERALL ASSESSMENT
Non-compliant calibration and control blank contamination data quality issues were found to impact the
results reported.
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DATA ASSESSMENT NARRATIVE FOR METALS
SITE: FCX Statesville
LABORATORY: Eckenfelder, Inc.
Validation Report: FCX299A
This sample delivery group consists of the following water samples:
W-31s W-31s Duoe EB I'll W-31i W-31i W-32i WoosterWell Hinson Well W-201·
W-311 W-121 W-31s W-AA W-AB AA 121798 W-24s W-5s
W-8i W-26i W-18s W-19s W-9s W-20D W-16s W-161
W-28i W-AD W-17s W-32i W-29i W-AC W-22s W-22i
W-AE W-1s W-20s W-30i W-10i WSi
The samples described above were analyzed for either total target analyte list metals or manganese and
iron as directed on the field COC. The analyses were performed based on methodologies outlined in the
USEPA CLP SOW 3/90.
"USEPA Contract Laboratory Program National Functional Guidelines for inorganic Data Review" (Feb.,
1994) were used to evaluate the data set.
All data are valid and acceptable except those analytes which have been qualified with a "J" (estimated),
or "R" (unusable). All action is detailed on the attached sheets.
Major Data Quality Issues
None.
Minor Data Quality Issues
/GP Serial Dilution -Two analytes had an observed percent deviation value that fell outside validation
acceptance limits during one ICP serial dilution determination. Sample results associated with
the non-compliant serial dilution determination have been qualified as estimated.
Two facts should be noted by all data users. First, the "R" flag means that the associated value is
unusable. In other words, due to significant QC problems, the analysis is invalid and provides no
information as to whether the compound is present or not. "R" values should not appear on data tables
even as a last resort. The second fact to keep in mind is that no analyte concentration, even if it has
passed all QC tests, is guaranteed to be accurate. Strict QC serves to increase confidence in data but
·:'"'."'"'°""!\"'~ / /
i~--t~n:/4~~
Diane Waldschmidt v
Date: c...7 /46 ": ---7---r-/--'--,'---'--,L,L-
Environmental Scientist/Director
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HOLDING TIME
The amount of an analyte in a sample can change with time due to chemical instability, degradation,
volatilization, etc. If the specified holding time is exceeded the data may not be valid. Those analytes in
the samples whose holding time has been exceeded will be qualified as estimated, or unusable when
grossly exceeded.
All analyses were completed well within acceptable holding times.
BLANK CONTAMINATION
Quality assurance blanks, method, trip, field, or rinse blanks are prepared to identify any contamination
which may have been introduced into the samples during sample preparation or field activity. Trip blanks
measure cross contamination during shipment. Field and rinse blanks measure cross contamination
during field operations.
Method Blank Contamination
Method blanks were evaluated at the proper frequency. The associated method blanks provided data
indicating no contamination was present.
Field or Rinse Blank Contamination
Rinse blank and equipment blank samples were collected on every other day during field sample
collection. Upon evaluation of the field and equipment blank data obtained, no analytes were found to
be present at levels above the CRDL in any associated field or equipment blank.
CALIBRATION
Satisfactory instrument calibration is established to ensure that the instrument is capable of producing
acceptable quantitative data. The initial calibration curve and its verification demonstrates that the
instrument is capable of giving acceptable performance at the beginning of the analytical sequence. The
continuing calibration verification standards provide information as to the continuing stability of the
calibration curve.
Correlation Coefficient
All calibrations associated with the data represented here demonstrated satisfactorily that all criteria were
met.
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Initial and Continuing Calibration Verification
All initial and continuing calibration verifications that bracketed sample analyses associated with the
sample delivery group were within acceptance limits.
Initial and Continuing Calibration Blanks
All initial and continuing calibration blanks were evaluated and none associated with reported sample
results had observed analyte concentrations greater than the reported detection limits (positive or
negative).
MATRIX SPIKE/MATRIX SPIKE DUPLICATE
The matrix spike/matrix spike duplicate is generated to determine the precision and accuracy of the
analytical method in a given matrix. The matrix spike percent recoveries may be used to qualify data.
Sample W-31s was analyzed as a matrix spike/matrix spike duplicate for total target analyte metals with
the exception of mercury. The result of this evaluation was that all elements had favorable precision and
accuracy indicators. No qualification was applied based on the matrix spike/matrix spike duplicate
analyses.
Samples W-20I and W-10I were analyzed as matrix spike/matrix spike duplicate pairs for iron and
manganese. Both analytical pairs had indicators for precision and accuracy within control limits.
MATRIX SPIKE
Samples W-31I, W-16I and AA121798 were selected for the mercury matrix spike analysis. All samples
had percent recoveries for mercury well within acceptable limits.
DUPLICATE
Samples EB@ W-31I, AA12179 and W-16I were performed in duplicate for mercury analysis. All
samples had observed relative percent difference values well within the allowable limit (20%). The
duplicate analysis for mercury performed on sample EB@ W-31 i was not appropriate. However, there
were other duplicate analyses associated with the analytical run. Therefore, no qualification of data was
applied.
A duplicate analysis was performed on sample W-31s for calcium, magnesium, potassium and sodium.
All analytes had relative percent difference values well within the allowable limit (20%).
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LABORATORY CONTROL SAMPLE
The Laboratory Control Sample is a quality control sample of known concentration which is processed
along with a batch of samples. The percent recovery of the LCS can be used to assess the accuracy of
the analytical procedure performed by a specific individual. during a specific time period, and utilizing the
same reagents and equipment as those used for sample analyses. The LCS data is independent of
sample matrix and the results may formulate a basis for qualification.
All associated laboratory control samples had observed percent recoveries well within the range
required.
ICP SERIAL DILUTION
Precision between diluted, and non-diluted analyses was determined on sample W-31s. All metal
analytes met validation acceptance limits with the exception of potassium (11.9%) and sodium (46.4%).
The following samples were associated with the serial dilution determination described above.
Potassium and sodium results for the samples listed have been flagged as estimated "J" or "UJ".
W-31S W-31S Du EB W-31i W-31i
W-32i Wooster Well Hinson Well
Precision between diluted and non-diluted analyses was determined on samples W-1 DI and W-20I for
iron and manganese only during two separate analytical runs. Both data sets had all percent deviation
values for iron and manganese within validation guidelines.
CRDL
CRDL (2 times the CRDL) standards were analyzed as required during ICP analytical run sequences
Upon evaluation two selenium (initial and final) and one thallium standard recovery were slightly higher
than the highest acceptable validation limit. The validator elected not to apply any optional qualifiers to
the data set based on the minor CRDL excursion.
INTERFERENCE CHECK STANDARDS
Interference check standard analyses were performed at the proper frequency. Upon examination the
recoveries of all standards were well within acceptable limits (80-120%) for both the initial and final
determinations.
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FIELD DUPLICATE
Samples W-31s and W-31s Dupe, W-31s and W-AA, W-24s and W-BB and W-29i and W-AC comprised
the field duplicate pairs associated with this sample delivery group. The following table lists the relative
percent difference values for each (positive at the CRDL results only) of the field duplicate pairs.
W-31s (11/19/98) RPD
Aluminum 129%
Calcium 40%
Iron 133%
Lead , , , %
Magnesium 97%
Manganese 49%
Sodium 16%
Zinc 136%
W-31s (12/16/98) RPD
Iron 7.7%
Manganese 0%
W-29i (12/20/98) RPD
Manganese 2.3%
SYSTEM PERFORMANCE AND OVERALL ASSESSMENT
The laboratory attempted to perform the analyses evaluated according to USEPA CLP SOW 3/90. The
following are procedural deficiencies not directly impacting data quality and therefore not previously
discussed.
1. No more than 20 field samples should be included in a single sample delivery group. This SDG
contains 25 environmental samples and four field blanks.
2. No unspiked duplicate was performed for all TAL metals as required by CLP methodologies.
Please note, samples analyzed for target analyte metals were acid digested using 50 ml of sample and a
final volume of 25 m I thereby increasing method sensitivity by a factor of 2. However, it should be
understood that per the analytical method a 100 ml aliquot should be digested with a final volume of 100
ml.
5
I
I
I
I
I
I
I
I
I
I
I
I'
I
I
I
I
I
I
I
u -
J -
R
N
JN -
UJ -
GLOSSARY OF DATA QUALIFIERS
The material was analyzed for, but not detected. The associated numerical value is the sample
quantitation limit.
The associated numerical value is an estimated quantity.
The data are unusable (compound may or may not be present).
Presumptive evidence of the presence of the material.
Presumptive evid_ence of the presence of the material at an estimated concentration.
The material was analyzed for, but was not detected. The sample quantitation limit is an
estimated quantity.
6
I
I
I
I
I
I
I LABORATORY DATA WITH QUALIFIERS ADDED
I
I
I
I
I
I
I
I
I
I
I
I
I
I 00078
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-20I
Name: ECKENFELDER INC. Contract: EL PASO
l ab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
.atrix: (soil/water) WATER
l ample wt/vol:
,evel: (low/med)
I Moisture: not dee.
25.00 (g/mL) ML
LOW
Lab Sample ID: 9812156-01
Lab File ID: 1215601D
Date Sampled: 12/15/98
Date Analyzed: 12/26/98
Dilution Factor: 50.0 C Column: DB-624 loil Extract Volume:
ID: 0.53 (mm)
(uL) ----Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
a
I
I
CAS NO. COMPOUND
67-64-1---------Acetone
71-43-2---------Benzene
.
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfiae
56-23-5---------Carbon tetrachlor1.ae
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
250
50
50
50
50
50
250
14
50
50
50
5
74-87-3---------Chloromethane So·➔
124-48-1--------Dibromochloromethane 50
96-12-8---------1,2-D~bromo-3-chloropropane_ 50
106-93-4--------1,2-Dibromoethane 50
95-50-1---------1,2-Dichlorobenzene 50
541-73-1--------1,3-Dichlorobenzene 50
106-46-7--------1,4-Dichlorobenzene 50
75-34-3---------1,1-Dichloroethane 50
107-06-2--------1,2-Dichloroethane 50
75-35-4---------1,1-Dichloroethene 50
156-59-2--------cis-l,2-Dichloroethene 120
156-60-5--------trans-l,2-Dichloroethene 50
78-87-5---------1,2-Dichloropropane --48
10061-01-5------cis-l,3-Dichloropropene 50
10061-02-6------trans-l,3-Dichloropropene __ 50
100-41-4--------Ethylbenzene 50
591-78-6--------2-Hexanone 250
75-09-2---------Methylene chloriae i ?'/}-'!,
108-10-1--------4-Methyl-2-pentanone 250
100-42-5--------Styrene 50
79-34-5---------1,1,2,2-Tetrachloroethane 50
127-18-4--------Tetrachloroethene --1100
108-88-3--------Toluene -5c,..:,,
*=SEE CASE NARRATIVE.
FORM I VOA
Q
UD
UD
UD
UD
UD
UD
UD
JD
UD
UD
UD
JD
-.ffiB
UD
UD*
UD
UD
UD
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UD
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UD
UD
UD
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J:lID.
UD
UD
UD
D
,IB-B-
: 1-41 d' J oiv
R.
f\
(/
R
(./
iJ
00079
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-20I
ECKENFELDER INC. Contract: EL PASO
t,ab ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
9'1atrix: (soil/water) WATER
'ample
Level:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812156-01
Lab File ID:
Date Sampled:
1215601D
12/15/98
Date Analyzed: 12/26/98
Dilution Factor: 50.0
Soil Aliquot Volume: toil Extract Volume: ____ (uL)
I
I
u
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
g
I
I
I
I
I
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
50 UD
50 UD
75 D
50 UD
50 UD
00093
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-31I
Name: ECKENFELDER INC. Contract: EL PASO
lab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
,atrix: (soil/water) WATER
fample wt/vol:
Level: (low/med)
25.00 (g/mL) ML
LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812156-02
Lab File ID: 1215602
Date Sampled: 12/16/98
Date Analyzed: 12/22/98
Dilution Factor: 1.0 toil Extract Volume: ____ (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
I
I
I
I
I
I
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
f
I
I
I
I
I
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disull'iae
56-23-5---------Carbon tetrachloriae
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans~l,2-Dichloroethene __
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloriae
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane
127-18-4--------Tetrachloroethene --
108-88-3--------Toluene
FORM I VOA
5.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
1.0 u
1. 0 u
1. 0 u
1.0 u
0.09 J
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
;J. 0 9-73--JB
5.0 u
1. 0 u
1. 0 u
0.1 J
I · 0 fr.fr! JB
I
u
I
I 00094
FORM 1 CLIENT SAMPLE NO. -I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-31I
Lab Name: ECKENFELDER INC. Contract: EL PASO
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER I ample wt/vol:
·Level: (low/med) t Moisture: not dee.
25.00 (g/mL) ML
LOW.
GC Column: DB-624 ID: 0.53 (mm) toil Extract Volume : ____ (uL)
Lab Sample ID: 9812156-02
Lab File ID: 1215602
Date Sampled: 12/16/98
Date Analyzed: 12/22/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
i
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
' I
,I
' I
I .,
I
a·
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
00102
I
I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-12I
ECKENFELDER INC. Contract: EL PASO
fab ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
'latrix: (soil/water) WATER
··ample
Level:
wt/vol:
(low/med)
25. 00 (g/rnL) ML
LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812156-03
Lab File ID:
Date Sampled:
1215603
12/16/98
Date Analyzed: 12/25/98
Dilution Factor: 1.0
,,oil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
'I' 1«
:J' J J;'tll I
I
I
I
I
I'
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
67-64-1---------Acetone 5.0 u
71-43-2---------Benzene 0.04 J
75-27-4---------Bromochloromethane 1.0 u
75-27-4---------Bromodichloromethane 1. 0 u
75-25-2---------Bromoforrn 1. 0 u
74-83-9---------Bromomethane 1.0 u
78-93-3---------2-Butanone 5.0 u
75-15-0---------Carbon disulfiae 0.05 J
56-23-5---------Carbon tetrachloriae 1.0 u
108-90-7--------Chlorobenzene 1.0 u
75-00-3---------Chloroethane 1.0 u
67-66-3---------Chloroforrn 0.3 J
74-87-3---------Chloromethane 1.0 u
124-48-1--------Dibromochloromethane i.O u
96-12-8---------1,2-Dibromo-3-chloropropane 1.0 u
106-93-4--------1,2-Dibromoethane -1.0 u
95-50-1---------1,2-Dichlorobenzene 1.0 u
541-73-1--------1,3-Dichlorobenzene 1.0 u
106-46-7--------1,4-Dichlorobenzene 1.0 u
75-34-3---------1,1-Dichloroethane 0.5 J
107-06-2--------1,2-Dichloroethane 1. 0 u
75-35-4---------1,1-Dichloroethene 0.2 J
156-59-2--------cis-1,2-Dichloroethene 1.0 u
156-60-5--------trans-1 2-Dichloroethene 1.0 u ' --78-87-5---------1,2-Dichloropropane 1.0 u
10061-01-5------cis-1,3-Dichloropropene 1.0 u
10061-02-6------trans-l,3-Dichloropropene __ 1.0 u
100-41-4--------Ethylbenzene 1.0 u
591-78-6--------2-Hexanone 5.0 u
75-09-2---------Methylene chlon.ae dJ-0 &,-r iJ-
108-10-1--------4-Methyl-2-pentanone 5.0 u
100-42-5--------Styrene 1. 0 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 1.0 u
127-18-4--------Tetrachloroethene 2
108-88-3--------Toluene / n nc .o ,T
FORM I VOA
((
u:r
I u
J'
u
I
I FORM 1
00103
CLIENT SAMPLE NO.
'Lab
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-12I
Name: ECKENFELDER INC. Contract: EL PASO rab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
·a.sample wt/vol:
Level: (low/med)
25.00 (g/mL) ML
LOW
1% Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812156-03
Lab File ID: 1215603
Date Sampled: 12/16/98
Date Analyzed: 12/25/98
Dilution Factor: 1.0
Soil Aliquot Volume: ,ISoil Extract Volume: ____ (uL)
CONCENTRATION UNITS:
·' I
1·
' I
' I ,.
i
u
I
I
1·
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
71-55-6---------1,1,1-Trichloroethane 1.0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 1.0 u
75-01-4---------Vinyl chloride 1.0 u
1330~20-7-------Xylene(total) 1.0 u
FORM I VOA
I
I
I
00115
FORM l CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-31S
Lab Name: ECKENFELDER INC. Contract: EL PASO fab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
., ample wt/vol:
Level: (low/med) t .Moisture: not dee.
25.00 (g/mL) ML
LOW
··Ge Column: DB 0 624 ID: 0.53 (mm)
Lab Sample ID: 9812156-04
Lab File ID: 1215604
Date Sampled: 12/16/98
Date Analyzed: 12/22/98
Dilution Factor: 1.0
1foil Extract Volume : ____ (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
I'
I
·1
I
I
1·
I
I'
I
I
' •.
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------carbon tetrachlon.de
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene --78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane
127-18-4--------Tetrachloroethene --
108-88-3--------Toluene
FORM I VOA
5.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
0.05 J
1.0 u
i. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
0.04 J
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
5.0 u
;;i..o e-:-s J-B-
5.0 u
1.0 u
1.0 u
1.0 u
I, o '07B4 7JJ,
JI.._
u
I
I· 00116
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
'ab Name: ECKENFELDER INC. Contract: EL PASO
W-31S
tab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
'lsample wt/vol:
Level: (low/med)
1% Moisture: not dee.
25.00 (g/mL) ML
LOW
·Ge Column: DB-624 ID: 0.53 (mm)
Extract Volume: ____ (uL)
Lab Sample ID: 9812156-04
Lab File ID: 1215604
Date Sampled: 12/16/98
Date Analyzed: 12/22/98
Dilution Factor: 1.0
Soil Aliquot Volume: 'Soil
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I ,.
/ I ,,,
f ,,
·1·
I
71-55-6---------1,1,1-Trichloroethane 1. 0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 1.0 u
75-01-4---------Vinyl chloride 1. 0 u
1330-20-7-------Xylene(total) 1. 0 u
FORM I VOA
.1
I
I
00124
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-AA
Lab Name: ECKENFELDER INC. Contract: EL PASO
·tab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
•tample wt/vol:
Level: (low/med)
25.00 (g/mL) ML
LOW t Moist~re: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812156-05
Lab File ID: 1215605
Date Sampled: 12/16/98
Date Analyzed: 12/22/98
Dilution Factor: 1.0
,, ,, ,,
I'
1·
I
I:
I
Extract Volume: ____ (uL) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1----~----Acetone 5.0
71-43-2---------Benzene 1,0
75-27-4---------Bromochloromethane 1.0
75-27-4---------Bromodichloromethane 1. 0
75-25-2---------Bromoform 1.0
74-83-9---------Bromomethane 1.0
78-93-3---------2-Butanone 5.0
75-15-0---------Carbon disull:iae 1.0
56-23-5---------Carbon tetrachloriae 1.0
108-90-7--------Chlorobenzene 1.0
75-00-3---------Chloroethane 1. 0
67-66-3---------Chloroform 0.04
74-87-3---------Chloromethane 1.0
124-48-1--------Dibromochloromethane 1.0
96-12-8---------1,2-Dibromo-3-chloropropane 1.0
106-93-4--------1,2-Dibromoethane -1.0
95-50-1---------1,2-Dichlorobenzene 1.0
541-73-1--------1,3-Dichlorobenzene 1.0
106-46-7--------1,4-Dichlorobenzene 1.0
75-34-3---------1,1-Dichloroethane 1.0
107-06-2--------1,2-Dichloroethane 1.0
75-35-4---------1,1-Dichloroethene 1.0
156-59-2--------cis-1,2-Dichloroethene 0.06
156-60-5--------trans-l,2-Dichloroethene 1. 0
78-87-5---------1,2-Dichloropropane --1.0
10061-01-5------cis-1,3-Dichloropropene 1.0
10061-02-6------trans-l,3-Dichloropropene 1. 0
100-41-4--------Ethylbenzene --1.0
591-78-6--------2-Hexanone 5.0
75-09-2---------Methylene chloriae -;;.o-o--:-s-
108-10-1--------4-Methyl-2-pentanone 5.0
100-42-5--------Styrene 1 .. 0
79-34-5---------1,1,2,2-Tetrachloroethane 1. 0
127-18-4--------Tetrachloroethene · --1.0
108-88-3--------Toluene i,Q-0-.M
FORM I VOA
u u u
u
u u u
u u u u
J u u u
u u u u
u u u
J
u u u u
u u
,ffi
u
u u u
JB.
IZ
I '.)
u
,,
00125
FORM 1 CLIENT SAMPLE NO. I'
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-AA
Lab Name: ECKENFELDER INC. Contract: EL PASO
'Jl,ab Code : NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water)
tample wt/vol:
Level: (low/med) t Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812156-05
Lab File ID: 1215605
Date Sampled: 12/16/98
Date Analyzed: 12/22/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL) toil Extract Volume: ____ (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
...
I
I
I
I
I\
-I
I
I'
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
4
FORM I VOA
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
I
' I,
00133
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-AB
Lab Name: ECKENFELDER INC. Contract: EL PASO
'tb Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER Lab Sample ID: 9812156-06
Lab File ID: 1215606
Date Sampled: 12/16/98
Date Analyzed: 12/23/98
Dilution Factor: 1.0
lample wt/vol: 25. 00 (g/mL) ML
Level: (low/med) LOW .. · .
.• Moisture: not dee.
' ' GC Column: DB-624 ID: 0.53 (mm)
Extract Volume: (uL) -----Soil Aliquot Volume:
I \..,I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulb.de
56-23-5---------carbon tetrachlon.de
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chlon.de
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane
127-18-4--------Tetrachloroethene --
108-88-3--------Toluene
FORM I VOA
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1. 0
1.0
1.0
1.0
0.1
i. 0
1.0
1. 0
1.0
1.0
1.0
1.0
1. 0
1.0
1. 0
1.0
1.0
1.0
1.0
1.0
5.0
0.9
5.0
1.0
1. 0
1.0
0.07
u u u u u
u u u u
u u·
u
J u u
u
u u u
u u u u
u u u u u u
JB u u u u
JB
r \
00134
FORM 1 CLIENT SAMPLE NO,
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-AB
Lab Name: ECKENFELDER INC. Contract: EL PASO
·1ab Code: NA Batch No. : NA SAS No.: NA SDG No,: FCX.Vl215601
·Matrix: (soil/water) WATER
'lample wt/vol: 25. 00 (g/mL) ML
Level: (low/med) LOW l Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
.,oil Extract Volume : ____ (uL)
Lab Sample ID: 9812156-06
Lab File ID: 1215606
Date Sampled: 12/16/98
Date Analyzed: 12/23/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
,'
I-
I'
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
I
00140
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ECKENFELDER INC. Contract: EL PASO
TRIP BLA
NK #1204
'lab Code : NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
~atrix: (soil/water)
,.ample wt/vol:
Level: (low/med)
,, Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812156-07
Lab File ID: 1215607
Date Sampled: 12/16/98
Date Analyzed: 12/23/98
Dilution Factor: 1.0 toil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
1. ,,
:I'
I
' I
,I
D,
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachlon.de
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene --78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
-100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --127-18-4--------Tetrachloroethene
108-88-3--------Toluene
FORM I VOA
5.0
1.0
1.0
1.0
1.0
1. 0
5.0
1.0
1. 0
1. 0
1.0
1.0
0.07
1. 0
1.0
1. 0
1.0
1.0
1.0
1. 0
1.0
1.0
1. 0
1.0
1.0
1.0
1.0
1. 0
5.0
0.7
5.0
1.0
1.0
1. 0
0.06
Q
u u
u u u u
u u u u u
u
J u
u u u u
u u u u
u u u
u
u u u
JB
u u
u u
JB
1A1
J' j Q/J';
"Z
uT
00141
FORM 1 CLIENT SAMPLE NO.
I
I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELDER INC. Contract: EL PASO
TRIP BLA
NK #1204
Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water)
liample wt/vol:
i;eve~: (low/med)
.. Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm) Jail Extract Volume : ____ (uL)
Lab Sample ID: 9812156-07
Lab File ID: 1215607
Date Sampled: 12/16/98
Date Analyzed: 12/23/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I ,,
1-
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
1.0 u
1.0 u
1.0 u
1. 0 u
1. 0 u
I
I
I
00147
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET HOLDING
BLANK 121798
Lab Name: ECKENFELDER INC. Contract: EL PASO
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER lample wt/vol: 25. 00 (g/mL) ML
'l,evel: (low/med) LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812156-08
Lab File ID: 1215608
Date Sampled: 12/17/98
Date Analyzed: 12/23/98
Dilution Factor: 1.0
loil Extract Volume: _____ (uL) Soil Aliquot Volume:
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------carbon disulb.de
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene --78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --127-18-4--------Tetrachloroethene
108-88-3--------Toluene
FORM I VOA
5.0
1.0
1. 0
1.0
1.0
1. 0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1. 0
1.0
1.0
1. 0
1.0
1. 0
1.0
1. 0
5.0
0.10
5.0
1. 0
1. 0
1.0
1. 0
u u u u u
u u u
u
u u u
u u u
u
u u u
u u u u
u u u u u u
JB
u
u u u u
rz
1...!T
00148
FORM 1 .CLIENT SAMPLE NO.
I
I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ECKENFELDER INC. Contract: EL PASO
HOLDING
BLANK 121798
lab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
lample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW B Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
11,oil Extract Volume: ____ (uL)
Lab Sample ID: 9812156-08
Lab File ID: 1215608
Date Sampled: 12/17/98
Date Analyzed: 12/23/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
71-55-6---------1,1,1-Trichloroethane 1. 0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 1.0 u
75-01-4---------Vinyl chloride 1. 0 u
1330-20-7-------Xylene(total) 1.0 u
FORM I VOA
I
I
I
Lab tab
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELDER INC. Contract: EL PASO
Code: NA Batch No.: NA SAS No.: NA
00152
CLIENT SAMPLE NO.
AA121798
SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER Lab Sample ID: 9812163-01
Lab File ID: 1216301D
Date Sampled: 12/17/98
Date Analyzed: 12/27/98
Dilution Factor: 50.0
Soil Aliquot Volume:
lample wt/vol:
Level: (low/med) I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Extract Volume: ____ (uL)
CAS NO. COMPOUND
67-64-1---------Acetone
71-43-2---------Benzene
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25c2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
250
4
50
50
50
50
250
50
50
50
50
50
50
50
50
50
50
50
50
290
50
100
I
I
I
I
I
I
I
I
I
I
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
I (;,[C -tttl-0
50
78-87-5---------1,2-Dichloropropane --50
10061-01-5------cis-l,3-Dichloropropene 50
10061°02-6------trans-l,3-Dichloropropene 50
100-41-4--------Ethylbenzene --50
591-78-6--------2-Hexanone 250
75-09-2---------Methylene chloride 100
108-10-1--------4-Methyl-2-pentanone 250
100-42-5--------Styrene 50
79-34-5---------1,1,2,2-Tetrachloroethane 50
127-18-4--------Tetrachloroethene --200
108-88-3--------Toluene 50
*=SEE CASE NARRATIVE.
FORM I VOA
Q
UD
JD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD*
UD
UD
UD
UD
D
UD
D
BE-.D
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
D
UD
00153
FORM 1 CLIENT SAMPLE NO.
I
I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
AA121798
Lab Name: ECK.ENFELDER INC. Contract: EL PASO
lab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
lample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm) Joil Extract Volume: ____ (uL)
Lab Sample ID: 9812163-01
Lab File ID: 1216301D
Date Sampled: 12/17/98
Date Analyzed: 12/27/98
Dilution Factor: 50.0
Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
71-55-6---------1,1,1-Trichloroethane 110 D
79-00-5---------1,1,2-Trichloroethane 10 JD
79-01-6---------Trichloroethene 67 D
75-01-4---------Vinyl chloride 26 JD
1330-20-7-------Xylene(total) so UD
FORM I VOA
I
I 00181
FORM 1 CLIENT SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-24S
Lab Name: ECKENFELDER INC. Contract: EL PASO
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER Lab Sample ID: 9812163-02
Lab File ID: 1216302
Date Sampled: 12/17/98
Date Analyzed: 12/22/98
Dilution Factor: 1.0
lample wt/vol:
Level: (low/med) I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Extract Volume: ____ (uL) Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone 5.0
71-43-2---------Benzene 0.1
75-27-4---------Bromochloromethane 1.0
75-27-4---------Bromodichloromethane 1.0
75-25-2---------Bromoform LO
74-83-9---------Bromomethane 1. 0
78-93-3---------2-Butanone 5.0
75-15-0---------Carbon disuir1.ae 1. 0
56-23-5---------Carbon tetrachlor1.ae 1.0
108-90-7--------Chlorobenzene 1. 0
75-00-3---------Chloroethane 1. 0
67-66-3---------Chloroform 0.09
74-87-3---------Chloromethane /, C ~
124-48-1--------Dibromochloromethane 1.0
96-12-8---------1,2-Dibromo-3-chloropropane_ 1.0
106-93-4--------1,2-Dibromoethane 1.0
95-50-1---------1,2-Dichlorobenzene 1. 0
541-73-1--------1,3-Dichlorobenzene 1.0
106-46-7--------1,4-Dichlorobenzene 1.0
75-34-3---------1,1-Dichloroethane 3
107-06-2--------1,2-Dichloroethane 1. 0
75-35-4---------1,1-Dichloroethene 3
156-59-2--------cis-l,2-Dichloroethene 7
156-60-5--------trans-l,2-Dichloroethene 0.4
78-87-5---------1,2-Dichloropropane --2
10061-01-5------cis-l,3-Dichloropropene 1. 0
10061-02-6------trans-l,3-Dichloropropene __ 1. 0
100-41-4--------Ethylbenzene 1.0
591-78-6--------2-Hexanone 5.0
75-09-2---------Methylene chior1.c!e ,;?,0 0--.-05
108-10-1--------4-Methyl-2-pentanone 5.0
100-42-5--------Styrene 1.0
79-34-5---------1,1,2,2-Tetrachloroethane 1. 0
127-18-4--------Tetrachloroethene --4o --6-6
108-88-3--------Toluene /,O ~
FORM I VOA
Q
u
J u u u u u u
u u u
J
-iJ-u
u u u u
u
u
J
J
u u
u u
1-JB-u
u u
% D
,ffi-
u
iZ.
i./
, u
00182
FORM 1 CLIENT SAMPLE NO.
I
I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-24S
Lab Name: ECKENFELDER INC. Contract: EL PASO
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER lample wt/vol: 25. 00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
l □il Extract Volume : ____ (uL)
Lab Sample ID: 9812163-02
Lab File ID: 1216302
Date Sampled: 12/17/98
Date Analyzed: 12/22/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
71-55-6---------1,1,1-Trichloroethane 1. 0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 12
75-01-4---------Vinyl chloride 0.1 J
1330-20-7-------Xylene(total) 1. 0 u
FORM I VOA
00212
I
I
I
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-5S
Lab Name: ECKENFELDER INC. Contract: EL PASO
lb Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V1215601
Matrix: (soil/water) WATER Lab Sample ID: 9812163-03
Jmple wt/vol: 25.00 (g/mL) ML Lab File ID: 1216303D
Level: (low/med) LOW Date Sampled: 12/17/98
I Moist~re: not dee. Date· Analyzed: 12/27/98
GC Column: DB-624 ID: 0.53 (mm) Dilution Factor: 200.0
.il Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone 1000
71-43-2---------Benzene 200
75-27-4---------Bromochloromethane 200
75-27-4---------Bromodichloromethane 200
75-25-2---------Bromoform 200
74-83-9---------Bromomethane 200
78-93-3---------2-Butanone 1000
75-15-0---------Carbon disulb.de 200
56-23-5---------Carbon tetrachloride 200
108-90-7--------Chlorobenzene 200
75-00-3---------Chloroethane 200
67-66-3---------Chloroform 200
74-87-3---------Chloromethane 200
124-48-1--------Dibromochloromethane 200
96-12-8---------1,2-D~bromo-3-chloropropane_ 200
106-93-4--------1,2-Dibromoethane 200
95-50-1---------1,2-Dichlorobenzene 200
541-73-1--------1,3-Dichlorobenzene 200
106-46-7--------1,4-Dichlorobenzene 200
75-34-3---------1,1-Dichloroethane 270
107-06-2--------1,2-Dichloroethane 200
75-35-4---------1,1-Dichloroethene 76
156-59-2--------cis-1,2-Dichloroethene 1600
156-60-5--------trans-1,2-Dichloroethene 200
78-87-5---------1,2-Dichloropropane --200
10061-01-5------cis-l,3-Dichloropropene 200
10061-02-6------trans-l,3-Dichloropropene 200
100-41-4--------Ethylbenzene --200
591-78-6--------2-Hexanone 1000
75-09-2---------Methylene chloride 400
108-10-1--------4-Methyl-2-pentanone 1000
100-42-5--------Styrene 200
79-34-5---------1,1,2,2-Tetrachloroethane 200
127-18-4--------Tetrachloroethene --;! 00 -14-0
108-88-3--------Toluene :;,. I} 0 . -"I
= SEE CASE NARRATIVE.
FORM I VOA
Q
UD
UD
UD
UD
UD
UD*
UD
UD
UD
UD
UD
UD
UD
UD
UD*
UD
UD
UD
UD
D
UD
JD
D
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
·-afr°
,HJ
:, < 1 ),:r1;,;
a.
V ::r
{
.J {
VJ
i rz
VJ
j
T :t V :;-
T
V J
-C ,y
:r (.)
I
I
I
00213
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-5S
Name: ECKENFELDER INC. Contract: EL PASO
Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
latrix: (soil/water)
ample wt/vol:
iilevel: (low/med)
I Moisture: not dee.
WATER
25. 00 (g/rnL) ML
LOW
,ac Column: DB-624 ID: 0.53 (mm)
loil Extract Volume: (uL) ----
Lab Sample ID: 9812163-03
Lab File ID: 1216303D
Date Sampled: 12/17/98
Date-Analyzed: 12/27/98
Dilution Factor: 200.0
Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
71-55-6---------1,1,1-Trichloroethane 85 JD
79-00-5---------1,1,2-Trichloroethane · 200 UD
79-01-6---------Trichloroethene 53 JD
75-01-4---------Vinyl chloride 50 JD
1330-20-7-------Xylene(total) 200 UD
FORM I VOA
j
V J
f
J V
I
I 00225
FORM 1 CLIENT SAMPLE NO.
I
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-8I
Lab Name: ECKENFELDER INC. Contract: EL PASO Jab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
tample wt/vol:
Level: (low/med) t Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812163-04
Lab File ID: 1216304
Date Sampled: 12/16/98
Date-Analyzed: 12/22/98
Dilution Factor: 1.0
toil Extract Volume: ____ (uL)
CAS NO. COMPOUND
Soil Aliquot Volume:
CONCENTRATION UNITS:
___ (uL)
/1'1' q 1
"J'~ or-tJ -(ug/L or ug/Kg) UG/L Q
..
67-64-1---------Acetone 44 J
71-43-2---------Benzene 0.08 J
75-27-4---------Bromochloromethane 1.0 u
75-27-4---------Bromodichloromethane 1. 0 u
75-25-2---------Bromoform 1. 0 u
74-83-9---------Bromomethane 1.0 u
78-93-3---------2-Butanone 5.0 u
75-15-0---------Carbon disulfide 0.5 J
56-23-5---------Carbon tetrachloride 1.0 u
108-90-7--------Chlorobenzene 1.0 u
75-00-3---------Chloroethane 1. 0 u
67-66-3---------Chloroform 1
74-87-3---------Chloromethane /.0 -0-c-5 -if u
124-48-1--------Dibromochloromethane 1.0 u
96-12-8---------1,2-Dibromo-3-chloropropane 1.0 u rz_
106-93-4--------1,2-Dibromoethane -1. 0 u
95-50-1---------1,2-Dichlorobenzene 1.0 u
541-73-1--------1,3-Dichlorobenzene 1.0 u
106-46-7--------1,4-Dichlorobenzene 1.0 u
75-34-3---------1,1-Dichloroethane 0.2 J
107-06-2--------1,2-Dichloroethane 1.0 u
75-35-4---------1,1-Dichloroethene 0.07 J
156-59-2--------cis-l,2-Dichloroethene 3
156-60-5--------trans-l,2-Dichloroethene --0.1 J
78-87-5---------1,2-Dichloropropane 5
10061-01-5------cis-l,3-Dichloropropene 1.0 u
10061-02-6------trans-l,3-Dichloropropene 1.0 u
100-41-4--------Ethylbenzene --0.04 J
591-78-6--------2-Hexanone 5.0 u
75-09-2---------Methylene chloride -;) • 0 -&-c-7 JB-u
108-10-1--------4-Methyl-2-pentanone 5.0 u
100-42-5--------Styrene 1. 0 u
79-34-5---------1,1,2,2-Tetrachloroethane --1.0 u
127-18-4--------Tetrachloroethene ·7 5 9-5 E+"
I
I
I
I
I
I
I
I
I
I
I
I
108-88-3--------Toluene 0 '9 ·/-'Cf)' -0-..-9-Jl3-J"6 , ;r
= T V SEE CASE NARRA IE.
FORM I VOA
I
I 00226
FORM 1 CLIENT SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-8I
Lab Name: ECKENFELDER INC. Contract: EL PASO
tab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
lample wt/vol:
Level: (low/med) I Moisture: not dee.
25.00 (g/mL) ML
LOW
GCColumn: DB-624 ID: 0.53 (mm)
loil Extract Volume : ____ (uL)
Lab Sample ID: 9812163-04
Lab File ID: 1216304
Date Sampled: 12/16/98
DateAnalyzed: 12/22/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
71-55-6---------1,1,1-Trichloroethane 1.0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 4
75-01-4---------Vinyl chloride 0.09 J
1330-20-7-------Xylene(total) 0.2 J
FORM I VOA
I
I 00248
FORM 1 CLIENT SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-18I
Lab Name: ECKENFELDER INC. Contract: EL PASO
.b Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
lample wt/vol: 25. 00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812163-04
Lab File ID: 1216304D
Date Sampled: 12/16/98
Date·Analyzed: 12/26/98
Dilution Factor: 5.0
loil
I
I
I
I
D
I
g
I
D
0
0
Extract Volume: ____ (uL) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone 82
71-43-2---------Benzene 5.0
75-27-4---------Bromochloromethane 5.0
75-27-4---------Bromodichloromethane 5.0
75-25-2---------Bromoform 5.0
74-83-9---------Bromomethane 5.0
78-93-3---------2-Butanone 25
75-15-0---------Carbon disull:ioe 5.0
56-23-5---------Carbon tetrachlorioe 5.0
108-90-7--------Chlorobenzene 5.0
75-00-3---------Chloroethane 5.0
67-66-3---------Chloroform 0.9
74-87-3---------Chloromethane 5,o-0.,.-4
124-48-1--------Dibromochloromethane 5.0
96-12-8---------1,2-Dibromo-3-chloropropane_ 5.0
106-93-4--------1,2-Dibromoethane 5.0
95-50-1---------1,2-Dichlorobenzene 5.0
541-73-1--------1,3-Dichlorobenzene 5.0
106-46-7--------1,4-Dichlorobenzene 5.0
75-34-3---------1,1-Dichloroethane 5.0
107-06-2--------1,2-Dichloroethane 5.0
75-35-4---------1,1-Dichloroethene 5.0
156-59-2--------cis-l,2-Dichloroethene 2.5
156-60-5--------trans~l,2-Dichloroethene __ 5.0
78-87-5---------1,2-Dichloropropane 4
10061-01-5------cis-l,3-Dichloropropene 5.0
10061-02-6------trans-l,3-Dichloropropene 5.0
100-41-4--------Ethylbenzene --5.0
591-78-6--------2-Hexanone 25
75-09-2---------Methylene cfilorioe 10
108-10-1--------4-Methyl-2-pentanone 25
100-42-5--------Styrene 5.0
79-34-5---------1,1,2,2-Tetrachloroethane __ 5.0
127-18-4--------Tetrachloroethene 61
108-88-3--------Toluene S:o-~
*=SEE CASE NARRATIVE.
FORM I VOA
Q
D.
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
JD
,JBf7"
UD
UD*
UD
UD
UD
UD
UD
UD
UD
JD
UD
JD
UD
UD
UD
UD
UD
UD
UD
UD
D
cfBB-
J
,1..
K.
u
fl._
Li
I
I 00249
FORM 1 CLIENT SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-18I
Lab Name: ECKENFELDER INC. Contract: EL PASO
lab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER lample wt/vol:
Level: (low/med) I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm) loil Extract Volume: ____ (uL)
Lab Sample ID: 9812163-04
Lab File ID: 1216304D
Date Sampled: 12/16/98
Date Analyzed: 12/26/98
Dilution Factor: 5.0
Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug'/Kg) UG/L Q
•
I
I
I
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
5.0 UD
5.0 UD
3 JD
5.0 UD
5.0 UD
I
I 00261
FORM 1 CLIENT SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-26I
Lab Name: ECKENFELDER INC. Contract: EL PASO
lab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER Lab Sample ID: 9812163-05
Lab File ID: 1216305
Date Sampled: 12/16/98
Date Analyzed: 12/25/98
Dilution Factor: 1.0
.ample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
foil Extract Volume: _____ (uL) Soil Aliquot Volume:
I
I
I
I
I
g
I
I
D
I
D
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulb.de
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane /, 0
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethan~
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-~8-6--------2-Hexanone
3
0.1
1.0
1.0
1. 0
1. 0
5.0
0.4
1. 0
1. 0
0.05
1.0
D.--3
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1. 0
1.0
0.03
1.0
1.0
1.0
1.0
0.1
5.0
75-09-2---------Methylene chloride .'.). C C-.-6-
108-10-1--------4-Methyl-2-pentanone 0.5
100-42-5--------Styrene 1.0
79-34-5---------1,1,2,2-Tetrachloroethane 1.0
127-18-4--------Tetrachloroethene --0.3
108-88-3--------Toluene 0.6
FORM I VOA
J
J
u u u u
u
J u u
J u
rrl' u u
u u u u
u u u
J u
u u u
J u
J.
J
u u
J
J
T
uT
u
V
:r
I
I FORM 1
00262
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET I Lab Name: ECKENFELDER INC. Contract: EL PASO
W-26I
fab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water)
fample wt/vol:
Level: (low/med)
WATER
25.00 (g/mL) ML
LOW t Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Extract Volume: ____ (uL)
Lab Sample ID: 9812163-05
Lab File ID: 1216305
Date Sampled: 12/16/98
Date Analyzed: 12/25/98
Dilution Factor: 1.0
Soil Aliquot Volume: foil
I
I
I
I
I
I
I
I
I
I
I
a
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
71-55-6---------1,1,1-Trichloroethane 1. 0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 0.09 J
75-01-4---------Vinyl chloride 0.2 J
1330-20-7-------Xylene(total) 0.5 J
FORM I VOA
I
I 00281
FORM 1 , CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
'ab Name: ECKENFELDER INC. Contract: EL PASO
W-18S
tb Code:. NA Batch No.: NA SAS No.: NA SDG No.: FCX0V1215601
Matrix: (soil/water) WATER Lab Sample ID: 9812163-06
tmple wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW
Lab File ID:
Date Sampled:
1216306
12/16/98
I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Extract Volume: ____ (uL)
Date Analyzed: 12/25/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
I
I
I
I
I
u
u
CAS NO. COMPOUND
67-64-1---------Acetone
71-43-2---------Benzene
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoforrn
74-83-9---------Bromomethane
78-93-3-------c-2-Butanone
75-15-0---------Carbon disull:iae
56-23-5---------Carbon tetrachloriae
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroforrn
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-1,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-1,3-Dichloropropene
10061-02-6------trans-1,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
5.0
1.0
1.0
1.0
1. 0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
i. 0
1. 0
1.0
1.0
1. 0
1.0
1. 0
1.0
1. 0
1.0
1.0
1. 0
1.0
1.0
1.0
5.0
75-09-2---------Methylene chloride ;z , C -l)_,..l,
108-10-1--------4-Methyl-2-pentanone 5.0
100-42-5--------Styrene 1.0
79-34-5---------1,1,2,2-Tetrachloroethane 1.0
127-18-4--------Tetrachloroethene --4
108-88-3--------Toluene /.0 ~
FORM I VOA
u u u u u
u u u
u u u
u u u u u u
u u u u
u u u
u u u
u u
·;;J·
u
u u
·cf
,,___
u
1./
00282
FORM 1 CLIENT SAMPLE NO.
I
I
I
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-18S
Lab Name: ECKENFELDER INC. Contract: EL PASO
Batch No. : NA lab Code: NA
Matrix: (soil/water) lample wt/vol:
SAS No.: NA SDG No.: FCX.V1215601
Level: (low/med)
WATER
25.00 (g/mL) ML
LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812163-06
Lab File ID: 1216306
Date Sampled: 12/16/98
Date Analyzed: 12/25/98
Dilution Factor: 1.0
Soil Aliquot Volume: toil Extract Volume: ____ (uL)
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
D
0
D
D
I
I
I
I
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7~------Xylene(total)
FORM I VOA
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
I
I FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
ECKENFELDER INC. Contract: EL PASO
00288
CLIENT SAMPLE NO.
W-19S
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
'latrix: (soil/water) WATER
lample
'tevel:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
ICMoisture: not dee.
~ Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812163-07
Lab File ID:
Date Sampled:
1216307
12/17/98
Date-Analyzed: 12/26/98
Dilution Factor: 1.0
I
I
I
I
I
D
0
I
m
E
I
I
Extract Volume: _____ (uL)
CAS NO. COMPOUND
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
___ (uL)
.. 1 /~ q
) p. 01.J Q
..
67-64-1---------Acetone 5.0 u
71-43-2---------Benzene 1.0 u
75-27-4---------Bromochloromethane 1. 0 u
75-27-4---------Bromodichloromethane 1. 0 u
75-25-2---------Bromoform 1. 0 u
74-83-9---------Bromomethane 1.0 u
78-93-3---------2-Butanone 5.0 u
75-15-0---------Carbon disull:1.ae 1. 0 u
56-23-5---------Carbon tetrachlor1.ae 0.3 J
108-90-7--------Chlorobenzene 1. 0 u
75-00-3---------Chloroethane 1.0 u
67-66-3---------Chloroform 1 J
74-87-3---------Chloromethane 1.0 u
124-48-1--------Dibromochloromethane 1. 0 u
96-12-8---------1,2-Dibromo-3-chloropropane_ 1.0 U*
106-93-4--------1,2-Dibromoethane 1.0 u
95-50-1---------1,2-Dichlorobenzene 1.0 u
541-73-1--------1,3-Dichlorobenzene 1. 0 u
106-46-7--------1,4-Dichlorobenzene 1.0 u
75-34-3---------1,1-Dichloroethane 1. 0 u
107-06-2--------1,2-Dichloroethane 1. 0 u
75-35-4---------1,1-Dichloroethene 0.3 J
156-59-2--------cis-l,2-Dichloroethene 4 u
156-60-5--------trans:l,2-Dichloroethene __ 0.05 J
78-87-5---------1,2-Dichloropropane 1
10061-01-5------cis-l,3-Dichloropropene 1.0 u
10061-02-6------trans-l,3-Dichloropropene __ 1.0 u
100-41-4--------Ethylbenzene 1.0 u
591-78-6--------2-Hexanone 5.0 u
75-09-2---------Methylene chlor1.ae ~-0 -e-:-3" JB-
108-10-1--------4-Methyl-2-pentanone 5.0 u
100-42-5--------Styrene 1. 0 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 1. 0 u
127-18-4--------Tetrachloroethene ;> 50 .;Rf) ·E-
108-88-3--------Toluene /. u --0-,-1 .JB.
(./
u
*=SEE CASE NARRATIVE.
FORM I VOA
I
I FORM 1
00289
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I W-19S
Lab Name: ECKENFELDER INC. Contract·: EL PASO
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
'ample wt/vol:
Level: (low/med)
25.00 (g/mL) ML
LOW t Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm) foil Extract Volume: ____ (uL)
Lab Sample ID: 9812163-07
Lab File ID:
Date Sampled:
1216307
12/17/98
Date· Analyzed: 12/26/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
D
0
0
I
I
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
1. 0 u
1.0 u
5
1.0 u
1.0 u
I
I FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
ECKENFELDER INC. Contract: EL PASO
00313
CLIENT SAMPLE NO.
W-9S
tab ~ode: NA Batch No. : NA
'atn.x: (soil/water) WATER
SAS No.: NA SDG No.: FCX.Vl215601
Lab Sample ID: 9812163-08
lample
,,evel:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
icMoisture: not dee.
t Column: DB-624 ID: 0.53 (mm)
Lab File ID:
Date Sampled:
1216308D
12/17/98
Date Analyzed: 12/23/98
Dilution Factor: 200.0
'oil Extract Volume : ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
D
CAS NO. COMPOUND
CONCENTRATION UNITS: 1-11
(ug/L or ug/Kg) UG/L Q ;~'J-Oiv'v
67-64-1---------Acetone 1000 UD
71-43-2---------Benzene 200 UD
75-27-4---------Bromochloromethane 200 UD
75-27-4---------Bromodichloromethane 200 UD
75-25-2---------Bromoform 200 UD
74-83-9---------Bromomethane 200 UD
78-93-3---------2-Butanone 1000 UD
75-15-0---------Carbon disulb.de 200 UD
56-23-5---------Carbon tetrachloride 200 UD
108-90-7--------Chlorobenzene 200 UD
75-00-3---------Chloroethane 200 UD
67-66-3---------Chloroform 200 UD
74-87-3---------Chloromethane ;200-:1.-4 crE)-u
124-48-1--------Dibromochloromethane 200 UD
96-12-8---------1,2-Dibromo-3-chloropropane 200 UD
106-93-4--------1,2-Dibromoethane -200 UD
95-50-1---------1,2-Dichlorobenzene 200 UD
541-73-1--------1,3-Dichlorobenzene 200 UD
106-46-7--------1,4-Dichlorobenzene 200 UD
75-34-3---------1,1-Dichloroethane 200 UD
107-06-2--------1,2-Dichloroethane 200 UD
75-35-4---------1,1-Dichloroethene 200 UD
156-59-2--------cis-1,2-Dichloroethene 200 UD
156-60-5--------trans-1,2-Dichloroethene 200 UD
78-87-5---------1,2-Dichloropropane --200 UD
10061-01-5------cis-1,3-Dichloropropene 200 UD
10061-02-6------trans-1,3-Dichloropropene 200 UD
100-41-4--------Ethylbenzene --200 UD
591-78-6--------2-Hexanone 1000 UD
75-09-2---------Methylene chloride i-ltJO -2-5-JB& u
108-10-1--------4-Methyl-2-pentanone 1000 UD
100-42-5--------Styrene 200 UD
79-34-5---------1,1,2,2-Tetrachloroethane 200 UD
127-18-4--------Tetrachloroethene --&ooo~o BE-"-l)
108-88-3--------Toluene 200 UD
*=SEE CASE NARRATIVE.
FORM I VOA
I
I FORM 1
00314
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
~ab Name: ECKENFELDER INC. Contract: EL PASO
W-9S
l,ab ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
~atrix: (soil/water) WATER
tample wt/vol:
Level: (low/med)
25.00 (g/mL) ML
LOW t Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812163-08
Lab File ID: 1216308D
Date Sampled: 12/17/98
Date Analyzed: 12/23/98
Dilution Factor: 200.0
Soil Aliquot Volume: ___ (uL) toil Extract Volume: ____ (uL)
CONCENTRATION UNITS:
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
71-55-6---------1,1,1-Trichloroethane . 200 UD
79-00-5---------1,1,2-Trichloroethane 200 UD
79-01-6---------Trichloroethene 24 JD
75-01-4---------Vinyl chloride 200 UD
1330-20-7-------Xylene(total) 200 UD
FORM I VOA
00333
I
I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
'ab Name: ECKENFELDER INC. Contract: EL PASO
W-20D
fi-b Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
fatrix: (soil/water) WATER Lab Sample ID: 9812163-09
tmple
Level:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
Lab File ID:
Date Sampled:
1216309
12/17/98 I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Date Analyzed: 12/25/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
I
I
Extract Volume: _____ (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L.
67-64-1---------Acetone 12
71-43-2---------Benzene 0.07
75-27-4---------Bromochloromethane 1.0
75-27-4---------Bromodichloromethane 1.0
75-25-2---------Bromoforrn 1.0
74-83-9---------Bromomethane 1.0
78-93-3---------2-Butanone 5.0
75-15-0---------Carbon disulb.de 1. 0
56-23-5---------Carbon tetrachloride 1.0
108-90-7--------Chlorobenzene 1.0
75-00-3---------Chloroethane 1.0
67-66-3---------Chloroform 1.0
74-87-3---------Chloromethane I. O 0.,.-,:-
124-48-1--------Dibromochloromethane 1. 0
96-12-8---------1,2-Dibromo-3-chloropropane 1.0
106-93-4--------1,2-Dibromoethane -1. 0
95-50-1---------1,2-Dichlorobenzene 1.0
541-73-1--------1,3-Dichlorobenzene 1.0
106-46-7--------1,4-Dichlorobenzene 1.0
75-34-3---------1,1-Dichloroethane 1. 0
107-06-2--------1,2-Dichloroethane 1.0
75-35-4---------1,1-Dichloroethene 0.03
156-59-2--------cis-l,2-Dichloroethene 0.02
156-60-5--------trans-l,2-Dichloroethene 3
78-87-5---------1,2-Dichloropropane --1
10061-01-5------cis-l,3-Dichloropropene 1.0
10061-02-6------trans-l,3-Dichloropropene 1.0
100-41-4--------Ethylbenzene --0.04
591-78-6--------2-Hexanone 5.0
75-09-2---------Methylene chloride J,00-.-2-
108-10-1--------4-Methyl-2-pentanone 0.4
100-42-5--------styrene 1.0
79-34-5---------1,1,2,2-Tetrachloroethane 1.0
127-18-4--------Tetrachloroethene --12
108-88-3--------Toluene 0.7
FORM I VOA
J
u u u u
u u u
u u u
J-
u u
u
u u u u
u
J
J
u
u
J u
,J-
J
u u
J
-J
L/.J
u
?Z
(..,'
T
I
I FORM 1
00334
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
~ab Name: ECKENFELDER INC. Contract: EL PASO
W-20D
tab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
fample wt/vol:
Level: (low/med)
25.00 (g/mL) ML
LOW t Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812163-09
Lab File ID: 1216309
Date Sampled: 12/17/98
Date Analyzed: 12/25/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL) foil Extract Volume: ____ (uL)
CONCENTRATION UNITS:
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
71-55-6---------1,1,1-Trichloroethane 1.0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 2
75-01-4---------Vinyl chloride 1. 0 u
1330-20-7-------Xylene(total) 0.2 J
FORM I VOA
I
I 00353
FORM 1 CLIENT SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-16S
-Lab Name: ECKENFELDER INC. Contract: EL PASO
fab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
lample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW ·t Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812163-10
Lab File ID: 1216310D
Date Sampled: 12/17/98
Date Analyzed: 12/27/98
Dilution Factor: 200.0
foil Extract Volume: ____ (uL) Soil Aliquot Volume: __ _;_(UL)
I
I
I
I
I
I
I
I
I
I
I
I
*
CAS NO. COMPOUND
67-64-1---------Acetone
71-43-2---------Benzene
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulriae
56-23-5---------Carbon tetrachloriae
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l 2-Dichloroethene ' --78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chloriae
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
SEE CASE NARRATIVE.
FORM I VOA
1000
200
200
200
200
200
1000
200
200
200
200
25
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
1000
400
1000
200
200
2300
200
Q
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
JD
UD
UD
UD*
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
D
UD
,,,,~'
r:). ,,-;~•'
fi.,
I
I FORM 1
00354
CLIENT SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-16S
Lab Name: ECKENFELDER INC. Contract: EL PASO
lab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V1215601
Matrix: (soil/water) WATER
lample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
loil Extract Volume : ____ (uL)
Lab Sample ID: 9812163-10
Lab File ID:
Date Sampled:
1216310D
12/17/98
Date Analyzed: 12/27/98
Dilution Factor: 200.0
Soil Aliquot Volume: ____ (uL)
I
I
I
I
I'
I
I
I
I
I
a
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
71-55-6---------1,1,1-Trichloroethane 200 UD
79-00-5---------1,1,2-Trichloroethane 200 UD
79-01-6---------Trichloroethene 40 JD
75-01-4---------Vinyl chloride 200 UD
1330-20-7-------Xylene(total) 200 UD
FORM I VOA
I
I
I
00360
FORM 1 .. CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-16I
Name: ECKENFELDER INC. Contract: EL PASO
Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
latrix: (soil/water)
ample wt/vol:
lilevel : (low/med)
'I. Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
Lab Sample ID: 9812163-11
Lab File ID: 1216311D
Date Sampled: 12/17/98
Date Analyzed: 12/22/98
Dilution Factor: 2.0
[
~c Column: DB-624 ID: 0.53 (mm)
il Extract Volume: ____ (uL) Soil Aliquot Volume: ----'-(uL)
I
I
I
I
I·
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
. (ug/L or ug/Kg) UG/L
67-64-1---------Acetone 10
71-43-2---------Benzene 2.0
75-27-4---·------Bromochloromethane 2.0
75-27-4---------Bromodichloromethane 3
75-25-2---------Bromoform 2.0
74-83-9---------Bromomethane 2.0
78-93-3---------2-Butanone 10
75-15-0---------Carbon disull:iae 2.0
56-23-5---------Carbon tetrachloriae SI./ -trB
108-90-7--------Chlorobenzene 2.0
75-00-3---------Chloroethane 2.0
67-66-3---------Chloroform .40
74-87-3---------Chloromethane ;:>-D~
124-48-1--------Dibromochloromethane 2.0
96-12-8---------1,2-Dibromo-3-chloropropane 2.0
106-93-4--------1,2-Dibromoethane -2.0
95-50-1---------1,2-Dichlorobenzene 2.0
541-73-1--------1,3-Dichlorpbenzene 0.2
106-46-7--------1,4-Dichlorqbenzene 0.2
75-34-3---------1,1-Dichloroethane 2.0
107-06-2--------1,2-Dichloroethane 0. 9
75-35-4---------1,1-Dichloroethene 0.4
78-87-5---------1,2-Dichloropropane 20
10061-01-5------cis-l,3-Dichloropropene 2.0
10061-02-6------trans-l,3-Dichloropropene 2.0
100-41-4--------Ethylbenzene --2.0
591-78-6--------2-Hexanone 10
75-09-2---------Methylene chloriae 1/,o.~
108-10-1--------4-Methyl-2-pentanone 10
100-42-5--------Styrene 2.0
79-34-5---------1,1,2,2-Tetrachloroethane 2.0
127-18-4--------Tetrachloroethene --/cM-,,-0-0-0
108-88-3--------Toluene ::J•O -0....2
FORM I VOA
Q ,,,;p·'I\
"" oi'I"
rz UD
UD
UD
D
UD
UD
UD
UD
BB-D
UD
UD
D ,re--u
UD
UD
UD
UD
JD
JD
UD
JD
JD
D
UD
UD
UD
UD
,ffifj-'
UD
UD
UD
-00 D
JBl,-u
00361
FORM l
I
I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
CLIENT SAMPLE NO.
W-16I
Name: ECKENFELDER INC. Contract: EL PASO
(
Lab
ab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
.Matrix: (soil/water)_
. Sample wt/vol:
ii.Leve~: (low/med)
% Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
IGC Column: DB-624 ID: 0.53 (mm)
·. Soil Extract Volume: ____ (uL)
Lab Sample ID: 9812163-ll
Lab File ID: 1216311D
Date Sampled: 12/17/98
Date Analyzed: 12/22/98
Dilution Factor: 2.0
Soil Aliquot Volume: ---'--(UL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I·
I
1·
I
I
I
I
I
71-55-6---------1,l,l-Trichloroethane
79-00-5----"----l,l,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
2.0 UD
2.0 UD
26 D
2.0 UD
2.0 UD
I
I 00393
FORM l CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name:
TRIP BLA
NK #1086*
ECKENFELDER INC. Contract: EL PASO
l ab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
atrix: (soil/water) WATER
13ample· wt/vol: 25.00 (g/mL) ML
LOW
Lab Sample ID: 9812163-12
Lab File ID: 1216312
Date Sampled: 12/17/98
Date Analyzed: 12/25/98
Dilution Factor: 1.0
'level: (low/med) I Moisture: not dee.
._,c Column: DB-624 ID: 0.53 (mm)
Extract Volume: ____ (uL) Soil Aliquot Volume:
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
. 75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulb.de
56-23-5---------Carbon tetrachlon.de
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,l-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,l-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene --78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chlon.de
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1 l 2 2-Tetrachloroethane ' ' ' --127-18-4--------Tetrachloroethene
108-88-3--------Toluene
FORM I VOA
5.0
LO
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
0.7
5.0
1.0
l. 0
0.2
0.05
u u
u u u u
u u u
u u u
u u u u u
u u u u
u u u u
u u u u
J u
u u
J
J
?..
i
..:.
I
I' ,
I
' I ' I ' '
\
j
J .. :J
1
+ J
J
I
I FORM 1
00394
CLIENT SAMPLE NO.
I
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ECKENFELDER INC. Contract: EL PASO
TRIP BLA
NK #1086 -X-
tb Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER Lab Sample ID: 9812163-12
lample wt/vol: 25.00 (g/mL) ML Lab File ID: 1216312
Level: (low/med) LOW Date Sampled: 12/17/98
I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Date Analyzed: 12/25/98
Dilution Factor: 1.0
'loil Extract Volume : ____ (uL)
CAS NO. COMPOUND
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
___ (uL)
:,_21-fo/
} . DJb-! Q
I
I
I
•
D
I
I
I
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
1.0 u I.IT
1.0 u
1. 0 u
1.0 u
1.0 u l
00401
I
I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELDER INC. Contract: EL PASO
HOLDING
BLANK 121898
lab ~ode: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
~trix: (soil/water) WATER
'
ample
evel:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
'C
Moisture: not dee.
Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812163-13
Lab File ID:
Date Sampled:
1216313
12/18/98
loil Extract Volume : _____ (uL)
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
Date Analyzed: 12/25/98
Dilution Factor: 1.0
Soil Aliquot Volume: ___ (uL)
·j,:11--4
t)/v'I
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
67-64-1---------Acetone 5.0 u fZ.
71-43-2---------Benzene 1.0 u
75-27-4---------Bromochloromethane 1.0 u
75-27-4---------Bromodichloromethane 1.0 u
75-25-2---------Bromoform 1.0 u
74-83-9---------Bromomethane 1. 0 u
78-93-3---------2-Butanone 5.0 u
75-15-0---------Carbon disull:iae 1. 0 u
56-23-5---------Carbon tetrachloriae 1.0 u 1/J
108-90-7--------Chlorobenzene 1.0 u
75-00-3---------Chloroethane 1.0 u
67-66-3---------Chloroform 1.0 u
74-87-3---------Chloromethane 1.0 u
124-48-1--------Dibromochloromethane 1.0 u
96-12-8---------1,2-Dibromo-3-chloropropane 1. 0 u
106-93-4--------1,2-Dibromoethane -1.0 u
95-50-1---------1,2-Dichlorobenzene 1.0 u
541-73-1--------1,3-Dichlorobenzene 1.0 u
106-46-7--------1,4-Dichlorobenzene 1.0 u
75-34-3---------1,1-Dichloroethane 1.0 u
107-06-2--------1,2-Dichloroethane 1.0 u
75-35-4---------1,1-Dichloroethene 1.0 u
156-59-2--------cis-l,2-Dichloroethene 1. 0 u
156-60-5--------trans-l,2-Dichloroethene 1.0 u
78-87-5---------1,2-Dichloropropane --1.0 u
10061-01-5------cis-l,3-Dichloropropene 1.0 u
10061-02-6------trans-l,3-Dichloropropene 1.0 u
100-41-4--------Ethylbenzene --1.0 u
591-78-6--------2-Hexanone 5.0 u
75-09-2---------Methylene chloriae 0.1 J
108-10-1--------4-Methyl-2-pentanone 5.0 u
100-42-5--------Styrene 1. 0 u
79-34-5---------1,1,2,2-Tetrachloroethane 1.0 u
127-18-4--------Tetrachloroethene --1.0 u I /J
108-88-3--------Toluene 1.0 u
FORM I VOA
D
I
I FORM 1
00402
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
~ab Name: ECKENFELDER INC. Contract: EL PASO
HOLDING
BLANK 121898
.Jab ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
~atrix: (soil/water) WATER
l3ample
'level:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812163-13
Lab File ID:
Date Sampled:
1216313
12/18/98
Date Analyzed: 12/25/98
Dilution Factor: 1.0
Soil Aliquot Volume: roil Extract Volume: ____ (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I
I
I
I
I
I
I
I
I
10
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
I
I
I
00406
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-28I
Lab Name: ECKENFELDER INC. Contract: EL PASO
tb· Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER Lab Sample ID: 9812176-01
Lab File ID: 1217601D
Date Sampled: 12/18/98
Date Analyzed: 12/22/98
Dilution Factor: 10.0
Soil Aliquot Volume:
lample wt/vol:
Level: (low/med) I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
.oil Extract Volume : ____ (uL)
CONCENTRATION UNITS:
I
I
I
I
I
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
0
I
I
I
I
I
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4-----~---Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulb.de
56-23-5---------Carbon tetrachlon.de
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene ,
79-34-5---------1,1,2,2-Tetrachloroethane
127-18-4--------Tetrachloroethene --
108-88-3--------Toluene
*=SEE CASE NARRATIVE.
FORM I VOA
50 UD
10 UD
10 UD
10 UD
10 UD
10 UD
50 UD
10 UD
2 JD
10 UD
10 UD
2 JD
ID G-c-8 .Jg..
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
10 UD
14 D
9 JD
10 UD
0.8 JD
10 UD
10 UD
10 UD
50 UD
J()--2 -a£f)"
50 UD
10 UD
10 UD
C, '-IC' %"fr E)E""l)
10 -fr.-4 i:fBB-
V
tJ
00407
I
I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
'1.ab Name: ECKENFELDER INC. Contract: EL PASO
W-28I
.ab ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
"r.iatrix: (soil/water) WATER
rample
Level:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW r Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812176-01
Lab File ID:
Date Sampled:
1217601D
12/18/98
Date Analyzed: 12/22/98
Dilution Factor: 10.0
Soil Aliquot Volume: roil Extract Volume : ____ (uL)
CONCENTRATION UNITS:
I
I
I
I
I
I
I
I
I
n
D
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
71-55-6---------1,1,1-Trichloroethane 10 UD
79-00-5---------1,1,2-Trichloroethane 10 UD
79-01-6---------Trichloroethene 24 D
75-01-4---------Vinyl chloride 10 UD
1330-20-7-------Xylene(total) 10 UD
FORM I VOA
I
I 00434
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET I W-AD
Lab Name: ECKENFELDER INC. Contract: EL PASO
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
'ample wt/vol:
Level: (low/med) I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812176-02
Lab File ID: 1217602
Date Sampled: 12/18/98
Date Analyzed: 12/27/98
Dilution Factor: 1.0
Extract Volume: _____ (uL) Soil Aliquot Volume: -----'--(uL)
I
I
I
I
I
I
I
D
0
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulb.de
56-23-5---------Carbon tetrachlon.de
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-D~bromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene --78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1 1 2 2-Tetrachloroethane ' ' ' --127-18-4--------Tetrachloroethene
108-88-3--------Toluene
= SEE CASE NARRATIVE.
FORM I VOA
Q
5.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 U* I
5.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1. 0 u
0.2 J
1.0 u
1. 0 U*
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u ' uT 1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
0.8 J
5.0 u
1.0 u
1.0 u
1.0 u
0.1 J
00435
I
I
I
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-AD
Lab Name: ECKENFELDER INC. Contract: EL PASO
lab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
lample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW
• Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm) Joil Extract Volume: ____ (uL)
Lab Sample ID: 9812176-02
Lab File ID: 1217602
Date Sampled: 12/18/98
Date Analyzed: 12/27/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
I
I
I
a
u
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
71-55-6---------1,1,1-Trichloroethane 1.0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene ,1.0 u
75-01-4---------Vinyl chloride 1.0 u
1330-20-7-------Xylene(total) 1.0 u
FORM I VOA
I
I 00441
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-17S
ECKENFELDER INC. Contract: EL PASO
W,ab ~ode: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
~atrix: (soil/water) WATER
l,ample
~evel:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW t Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812176-03
Lab File ID:
Date Sampled:
1217603
12/18/98
Date Analyzed: 12/31/98
Dilution Factor: 10000.0
,~il Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
67-64-1---------Acetone 50000 UD
71-43-2---------Benzene 10000, UD
75-27-4---------Bromochloromethane 10000 UD
75-27-4---------Bromodichloromethane 10000 UD
75-25-2---------Bromoform 10000 UD
74-83-9---------Bromomethane 10000 UD*
78-93-3---------2-Butanone 50000 UD
75-15-0---------Carbon disulfide 10000 UD
56-23-5---------Carbon tetrachloride 10000 UD
108-90-7--------Chlorobenzene 10000 UD
75-00-3---------Chloroethane 10000 UD
67-66-3---------Chloroform 10000 UD
74-87-3---------Chloromethane 10000 UD
124-48-1--------Dibromochloromethane 10000 UD
96-12-8---------1,2-Dibromo-3-chloropropane 10000 UD*
106-93-4--------1,2-Dibromoethane -10000 UD
95-50-1---------1,2-Dichlorobenzene 10000 UD
541-73-1--------1,3-Dichlorobenzene 10000 UD
106-46-7--------1,4-Dichlorobenzene 10000 UD
75-34-3---------1,1-Dichloroethane 10000 UD
107-06-2--------1,2-Dichloroethane 10000 UD
75-35-4---------1,1-Dichloroethene i() 0()6 1-3-0-B JBB-
156-59-2--------cis-l,2-Dichloroethene 10000 UD
156-60-5--------trans-l,2-Dichloroethene 10000 UD
78-87-5---------1,2-Dichloropropane --10000 UD
10061-01-5------cis-l,3-Dichloropropene 10000 UD
10061-02-6------trans-l,3-Dichloropropene 10000 UD
100-41-4--------Ethylbenzene --10000 UD
591-78-6--------2-Hexanone 50000 UD
75-09-2---------Methylene chloride .;JO C'C'O .............
vv v~
108-10-1--------4-Methyl-2-pentanone 50000 UD
100-42-5--------Styrene 10000 UD
79-34-5---------1,1,2,2-Tetrachloroethane --10000 UD
127-18-4--------Tetrachloroethene 72000 D
108-88-3--------Toluene 10000 UD
-SEE CASE NARRATIVE. -
FORM I VOA
,,-1, 1 I
I'\ t"C-•
0 r,i'J
rz
V vJ
I
I FORM 1.
00442
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: ECKENFELDER INC. Contract: EL PASO
W-17S
.ab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
~atrix: (soil/water) WATER
.ample
'level:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
ltCMoisture: not dee.
~ Column: DB-624 ID: 0.53 (mm)
Extract Volume: ____ (uL)
Lab Sample ID: 9812176-03
Lab File ID:
Date Sampled:
1217603
12/18/98
Date Analyzed: 12/31/98
Dilution Factor: 10000.0
Soil Aliquot Volume: ____ (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I
I
I
I
I
I
I
I
I
I
I
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
10000 UD
10000 UD
10000 UD
10000 UD
10000 UD
I
I 00450
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-32I
ECKENFELDER INC. Contract: EL PASO
jab ~ode: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
'1atrix: (soil/water) WATER
'ample wt/vol:
Level: (low/med) I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812176-04
Lab File ID: 1217604
Date Sampled: 12/18/98
Date Analyzed: 12/31/98
Dilution Factor: 1.0
.oil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
67-64-1---------Acetone 5.0 u
71-43-2---------Benzene I, 0 ~-,.JB-
75-27-4---------Bromochloromethane 1.0 u
75-27-4---------Bromodichloromethane 1.0 u
75-25-2---------Bromoform 1.0 u
74-83-9---------Bromomethane 1. 0 U*
78-93-3---------2-Butanone 5.0 u
75-15-0---------Carbon disulfide 1.0 u
56-23-5---------Carbon tetrachloride 1.0 u
108-90-7--------Chlorobenzene 1.0 u
75-00-3---------Chloroethane 1.0 u
67-66-3---------Chloroform 1. 0 u
74-87-3---------Chloromethane 1.0 u
124-48-1--------Dibromochloromethane 1. 0 u
96-12-8---------1,2-D~bromo-3-chloropropane_ 1.0 U*
106-93-4--------1,2-Dibromoethane 1.0 u
95-50-1---------1,2-Dichlorobenzene 1. 0 u
541-73-1--------1,3-Dichlorobenzene 1.0 u
106-46-7--------1,4-Dichlorobenzene 1.0 u
75-34-3---------1,1-Dichloroethane 1.0 u
107-06-2--------1,2-Dichloroethane 1.0 u
75-35-4---------1,1-Dichloroethene I • 0 4-.--,, ~
156-59-2--------cis-1,2-Dichloroethene 1.0 u
156-60-5--------trans-l,2-Dichloroethene 1.0 u --78-87-5---------1,2-Dichloropropane 1.0 u
10061-01-5------cis-1,3-Dichloropropene 1.0 u
10061-02-6------trans-1,3-Dichloropropene __ 1.0 u
100-41-4--------Ethylbenzene 1.0 u
591-78-6--------2-Hexanone 5.0 u
75-09-2---------Methylene chloride .;J' ll--G-;--5 ·a-
108-10-1--------4-Methyl-2-pentanone 5.0 u
100-42-5--------Styrene 1.0 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 1.0 u
127-18-4--------Tetrachloroethene 0.4 J
108-88-3--------Toluene i · 0 .()...,..,1.. J-
FORM I VOA
'
•1, t7,?f
cl l'M/
I<..
V UT
</T
fl....
u VJ
I
I
FORMl
00451
CLIENT SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-32I
'Lab Name: ECKENFELDER INC. Contract: EL PASO
tab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V1215601
Matrix: (soil/water) WATER
tample wt/vol:
Level: (low/med) t Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
toil Extract Volume: ____ (uL)
Lab Sample ID: 9812176-04
Lab File ID: 1217604
Date Sampled: 12/18/98
Date Analyzed: 12/31/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
71-55-6---------1,1,1-Trichloroethane 1. 0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 0.2 J
75-01-4---------Vinyl chloride 1.0 u
1330-20-7-------Xylene(total) 1.0 u
FORM I VOA
I
I FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
~ab Name: ECKENFELDER INC. Contract: EL PASO
00462
CLIENT SAMPLE NO.
TRIP BLA
NK #1101 I ;J.(J Cf
tab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
tample wt/vol:
Level: (low/med)
25.00 (g/mL) ML
LOW t Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812176-05
Lab File ID: 1217605
Date Sampled: 12/18/98
Date Analyzed: 12/27/98
Dilution Factor: ·1.0
I
I
I
I
I
I
I
I
I
I
g
0
Extract Volume: _____ (uL) Soil Aliquot Volume:
*
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulb.de
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene --78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane
127-18-4--------Tetrachloroethene --
108-88-3--------Toluene
SEE CASE NARRATIVE.
FORM I VOA
5.0
1.0
1. 0
1.0
1.0
1.0
5.0
1. 0
1. 0
1.0
1.0
1.0
1.0
1.0
1. 0
1.0
1.0
1.0
1.0
1.0
1.0
1. 0
1.0
1.0
1.0
1.0
1.0
1. 0
5.0
1
5.0
1. 0
1.0
1.0
0.04
u u u u u
U* u u
u u u
u
u u
U*
u u u u
u u u u
u u u
u u u
J u u
u u
J
!<.,
f/.. . I ;;-
t-._
J
)
u :r
I
I
FORM 1
00463
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELDER INC. Contract: EL PASO
TRIP BLA
NK #1184
Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
Jmple wt/vol: 25.00 (g/mL) ML
Levei: (low/med) LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Extract Volume: ____ (uL)
Lab Sample ID: 9812176-05
Lab File ID: 1217605
Date Sampled: 12/18/98
Date Analyzed: 12/27/98
Dilution Factor: 1.0
Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I
I
D
u
I
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
1.0 u
1. 0 u
1. 0 u
1. 0 u
1. 0 u
I
I
I
Lab
fab
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELDER INC. Contract: EL PASO
Code: NA Batch No.: NA SAS No.: NA
00468
CLIENT SAMPLE NO.
HOLDING
BLANK 122198
SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER Lab Sample ID: 9812176-06
Lab File ID: 1217606
Date Sampled: 12/21/98
Date Analyzed: 12/27/98
Dilution Factor: 1.0
lample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
loil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
CONCENTRATION UNITS:
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disuiriae
56-23-5---------Carbon tetrachloriae
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-D~bromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene __
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chloriae
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane
127-18-4--------Tetrachloroethene --
108-88-3--------Toluene
*; SEE CASE NARRATIVE.
FORM I VOA
5.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 U*
5.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1. 0 u
1.0 U*
1. 0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
0.1 J
5.0 u
1.0 u
1.0 u
1.0 u
1.0 u
~ 1/J .
I<.
rz.
v:r
I
I 00469
FORM 1 CLIENT SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ECKENFELDER INC. Contract: EL PASO
HOLDING
BLANK 122198
lab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
fample wt/vol: 25.00 (g/rnL) ML
Level: (low/med) LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm) loil Extract Volume: ____ (uL)
Lab Sample ID: 9812176-06
Lab File ID: 1217606
Date Sampled: 12/21/98
Date Analyzed: 12/27/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
71-55-6---------1,1,1-Trichloroethane 1. 0 u
79-00-5---------1,1,2-Trichloroethane 1. 0 u
79-01-6---------Trichloroethene 1.0 u
75-01-4---------Vinyl chloride 1.0 u
1330-20-7-------Xylene(total) 1.0 u
FORM I VOA
I
I FORM 1
00472A
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
'ab Name: ECKENFELDER INC. Contract: EL PASO
W-30I
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V1215601
Matrix: (soil/water) WATER Lab Sample ID: 9812182-01
Lab File ID: 1218201D
Date Sampled: 12/19/98
Date Analyzed: 12/23/98
Dilution Factor: 20.0
Soil Aliquot Volume:
'ample wt/vol:
Level: (low/med)
25.00 (g/mL) ML
LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm) toil Extract Volume : ____ (uL)
CONCENTRATION UNITS:
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
67-64-1---------Acetone 100 UD
71-43-2---------Benzene 20 UD
75-27-4---------Bromochloromethane 20 UD
75-27-4---------Bromodichloromethane 20 UD
75-25-2--.-- - - - --Bromoform 20 UD
74-83-9---------Bromomethane 20 UD
78-93-3---------2-Butanone 100 UD
75-15-0---------carbon disulfide 20 UD
56-23-5---------Carbon tetrachloride 20 UD
108-90-7--------Chlorobenzene 20 UD
75-00-3---------Chloroethane 20 UD
67-66-3---------Chloroform 20 UD
74-87-3---------Chloromethane .;::;o-2--.:fir
124-48-1--------Dibromochloromethane 20 UD
96-12-8---------1,2-D~bromo-3-chloropropane_ 20 UD
106-93-4--------1,2-Dibromoethane 20 UD
95-50-1---------1,2-Dichlorobenzene 20 UD
541-73-1--------1,3-Dichlorobenzene 20 UD
106-46-7--------1,4-Dichlorobenzene 20 UD
75-34-3---------1,1-Dichloroethane 20 UD
107-06-2--------1,2-Dichloroethane 20 UD
75-35-4---------1,1-Dichloroethene ;20 ➔ JB-
156-59-2--------cis-1,2-Dichloroethene 28 JD
156-60-5--------trans-1,2-Dichloroethene --20 UD
78-87-5---------1,2-Dichloropropane 5 JD
10061-01-5------cis-1,3-Dichloropropene 20 UD
10061-02-6------trans-1,3-Dichloropropene __ 20 UD
100-41-4--------Ethylbenzene 20 UD
591-78-6--------2-Hexanone 100 UD
75-09-2---------Methylene chloride L, 0 -3-,3'Bf)
108-10-1--------4-Methyl-2-pentanone 100 UD
100-42-5--------Styrene 20 UD
79-34-5---------1,1,2,2-Tetrachloroethane __ 20 UD
127-18-4--------Tetrachloroethene Sto6-ztl -BE-,::,
108-88-3--------Toluene ;;, 0 + JBu
FORM I VOA
(;,
u
f,
Cf7-u
u
J
u
I
I FORM 1
00473
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
~ab Name: ECKENFELDER INC. Contract: EL PASO
W-30I
S,ab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
l\atrix: (soil/water) WATER
l,ample
"level:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW r Moisture: not dee.
GC Column: DB-624 ID: 0.53 {mm)
Lab Sample ID: 9812182-01
Lab File ID:
Date Sampled:
1218201D
12/19/98
Date Analyzed: 12/23/98
Dilution Factor: 20.0 toil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
71-55-6---------1,1,1-Trichloroethane 20 UD
79-00-5---------1,1,2-Trichloroethane 20 UD
79-01-6---------Trichloroethene 46 D
75-01-4---------Vinyl chloride 20 UD
1330-20-7-------Xylene(total) 20 UD
FORM I VOA
'\"i.~
?.'~ C)
00495
I
I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-l0I
Name: ECKENFELDER INC. Contract: EL PASO
ILab ~ode: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V1215601
Matrix: (soil/water) WATER Lab Sample ID: 9812182-02
.Sample
Level:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
Lab File ID:
Date Sampled:
1218202
12/19/98
1% Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Date Analyzed: 12/31/98
Dilution Factor: 1.0
Soil Aliquot Volume: .Soil Extract Volume: ____ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
I
I
I
I
I
I
I
I
I
I
I
I
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disull:icle
56-23-5---------Carbon tetrachloricle
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene /, 0
156-59-2--------cis-1,2-Dichloroethene
156-60-5--------trans-1 2-Dichloroethene . ' --78-87-5---------1,2-Dichloropropane
10061-01-5-- - - --cis-1, 3 -Dichlorop·ropene
10061-02-6------trans-1,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chloricle C::J, C
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane ·
127-18-4--------Tetrachloroethene --
108-88-3--------Toluene
= SEE CASE NARRATIVE.
** SAMPLE PH EXCEEDED 2
SEE CASE NARRATIVE.
\ WHEN CHECKED BEFORE ANALYSIS.
FORM I VOA
5.0 u
1.0 U**
1. 0 u
1. 0 u
1.0 u
1.0 U*
5.0 u
1.0 u
1.0 u
1.0 U**
1. 0 u
1.0 u
1.0 u i.o u
1. 0 U*
1.0 u
1.0 U**
1.0 U**
1.0 U**
1. 0 u
1.0 u
-B7i ·,Jg
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 U**
5.0 u
~ 1-J--
5.0 u
1.0 u
1.0 u
2
1. 0 U**
u vr
!iT"
VY
,J.T
V.7
U.J
I
I 00496
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: ECKENFELDER INC. Contract: EL PASO
W-l0I
tab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water)
tample wt/vol:
Level: (low/med)
WATER
25.00 (g/mL) ML
LOW
1% Moisture: not dee.
. GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812182-02
Lab File ID: 1218202
Date Sampled: 12/19/98
Date Analyzed: 12/31/98
Dilution Factor: 1.0 toil Extract Volume: ____ (uL) Soil Aliquot Volume: --~(uL)
I
I
I
I
I
I
I
I
I
I
I
I
**
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
SAMPLE PH EXCEEDED 2 WHEN CHECKED BEFORE ANALYSIS.
SEE CASE NARRATIVE.
FORM I VOA
Q
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 U** VJ
00504
I
I FORM l CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: ECKENFELDER INC. Contract: EL PASO
W-5I
l b Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl21560l
, trix: (soil/water) WATER Lab Sample ID: 9812182-03
I. mple
vel:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
Lab File ID:
Date Sampled:
1218203
12/19/98
■Moisture: not dee.
~ Column: DB-624 ID: 0.53 (mm)
Extract Volume: ____ (uL)
Date Analyzed: 01/01/99
Dilution Factor: l.0
Soil Aliquot Volume:
I
I
D
I:
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene /.o
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7---~----Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-D~bromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,l-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,l-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-1,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride ~.U
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1 1 2 2-Tetrachloroethane , , , --
.5.0
~2
l.0
l. 0
1.0
1.0
5.0
l.0
l. 0
1.0
l. 0
0.06
1.0
1.0
l.0
1.0
1.0
1.0
1.0
5
1.0
4
10
1. 0
1.0
1.0
l.0
1.0
5.0 --
5.0
1. 0
1.0
127-18-4--------Tetrachloroethene .;)..T "2"9"
108-88-3--------Toluene 0.4
*=SEE CASE NARRATIVE.
FORM I VOA
Q
u
,J-
U* u u
U* u
u u u
u
J u u
U* u u u
u
u
u u u
u u u
JB-u
u u
-E D
J
A
~ T
~
g;
<
T
T
v 'T
00505
I
I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I · Lab Name: ECKENFELDER INC. Contract : EL PASO
W-5I
11,ab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V1215601
~atrix: (soil/water) WATER
.Sample
Level:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
1% Moisture: not dee.
GC Column: DB-624 ID: 0.5Z (mm)
Lab Sample ID: 9812182-03
Lab File ID:
Date Sampled:
1218203
12/19/98
Date Analyzed: 01/01/99
Dilution Factor: 1.0
Soil Aliquot Volume: I Soil Extract Volume : ____ (uL)
CONCENTRATION UNITS:
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
71-55-6---------1,1,1-Trichloroethane 1. 0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 4
75-01-4---------Vinyl chloride 0.3 J
1330-20-7-------Xylene(total) 0.02 J
FORM I VOA
00536
I
I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: ECKENFELDER INC. Contract: EL PASO
W-29I
a,ab ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
~atrix: (soil/water) WATER
iifample
'level:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
_[l"CMoisture: not dee.
~ Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812182-04
Lab File ID:
Date Sampled:
1218204D
12/20/98
Date Analyzed: 01/01/99
Dilution Factor: 2.0
roil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I.
I
I
CAS NO. COMPOUND
67-64-1---------Acetone
71-43-2---------Benzene
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfioe
56-23-5---------Carbon tetrachlorioe
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-D~bromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans~l,2-Dichloroethene __
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
10
2.0
2,0
2.0
2.0
2.0
10
2.0
0.4
2.0
2.0
1
2.0
2.0
2.0
2.0
2.0
2.0
2.0
4
2.0
3
7
2. 0
2.0
2.0
2.0
2.0
10 591-78-6--------2-Hexanone
75-09-2---------Methylene chlorioe 4,0--'I:-
108-10-1--------4-Methyl-2-pentanone 10
100-42-5--------Styrene 2.0
79-34-5---------1,1,2,2-Tetrachloroethane 2.0
127-18-4--------Tetrachloroethene --32
108-88-3--------Toluene 2.0
*=SEE CASE NARRATIVE.
FORM I VOA
Q
UD ~
UD
UD* u _,_
J
UD
UD
UD* iJ T
UD fl,.
UD
JD
UD
UD
JD
UD 'J
T_
.J
UD
UD* A_
UD
UD
UD
UD
D t
UD
D
D -
UD
UD
UD
UD
UD
UD
-OED" VT
UD
UD
UD
D J UD
D
I FORM 1
00537
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-29I
Name: ECKENFELDER INC. Contract: EL PASO
tab ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
atrix: (soil/water) WATER
j,ample
~evel:
wt/vol:
(low/med)
25. 00 (g/mL) ML
LOW t Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Extract Volume: ____ (uL)
Lab Sample ID: 9812182-04
Lab File ID:
Date Sampled:
1218204D
12/20/98
Date Analyzed: 01/01/99
Dilution Factor: 2.0
Soil Aliquot Volume: ____ (uL)
I
1,
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
' I
'I
I
I
I
I
I
71-55-6---------1,1,1-Trichlo!Oethane 2.0 UD
79-00-5---------1,1,2-Trichloroethane 2.0 UD
79-01-6---------Trichloroethene 2 JD
75-01-4---------Vinyl chloride 0.2 JD
1330-20-7-------Xylene(total) 2.0 UD
FORM I VOA
I
I 00551
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: ECKENFELDER INC. Contract: EL PASO
W-AC
i!,ab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V1215601
~atrix: (soil/water) WATER
.ample wt/vol:
l\evel: (low/med)
25.00 (g/mL) ML
LOW
_lfCMoisture: not dee.
~ Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812182-05
Lab File ID: 1218205D
Date Sampled: 12/20/98
Date Analyzed: 01/01/99
Dilution Factor: 2.0
I
I'
I
I'
'I•
l
I . ,
I
I
Extract Volume: (uL) ----Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4-------C-Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulb.de
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene '
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-1,2-Dichloroethene
156-60-5--------trans-1,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
.. 10
2.0
2.0
2.0
2.0
2.0
10
2.0
2.0
2.0
2.0
1
2.0
2.0
2.0
2.0
2.0
2.0
2.0
5
2.0
4
7
2. 0
2.0
2.0
2. 0
2.0
10
75-09-2---------Methylene chloride 4 , o__.,-
108-10-1--------4-Methyl-2-pentanone 10
100-42-5--------Styrene 2. 0
79-34-5---------1,1,2,2-Tetrachloroethane 2.0
127-18-4--------Tetrachloroethene --34
108-88-3--------Toluene 2.0
= SEE CASE NARRATIVE.
FORM I VOA
UD
UD
UD*.
UD
UD
UD*
UD
UD
UD
UD
UD
JD
UD
UD
UD*
UD
UD
UD
UD
D
UD
D
D
UD
UD
UD
UD
UD
UD
.JB&-
UD
UD
UD
D
UD
R.
u T
i) T ,,
'\
T a-
I:!..
fT
T
u T
j
I
00552
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-AC
Name: ECKENFELDER INC. Contract: EL PASO
l 1
ab ~ode: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
tatrix: (soil/water) WATER
j,ample
l!evel:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812182-05
Lab File ID:
Date Sampled:
1218205D
12/20/98
Date Analyzed: 01/01/99
Dilution Factor: 2.0
Soil Aliquot Volume: ----toil Extract Volume: ____ (uL)
I
I
I,
CAS NO. . COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
71-55-6---------1,1,1-Trichloroethane 2.0 UD
79-00-5---------1,1,2-Trichloroethane 2.0 UD
79-01-6---------Trichloroethene 2 JD
75-01-4---------Vinyl chloride 0.2 JD
1330-20-7-------Xylene(total) 2.0 UD
I'
FORM I VOA
I
(uL)
I
I
Ii
00565
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-22S
Lab Name: ECKENFELDER INC. Contract: EL PASO
fib Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
Jmple wt/vol: 25. 00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
,i:o::::c:B~:::me:_I_D_:_0 ___ 5:uL:mm)
Lab Sample ID: 9812182-06
Lab File ID: 1218206
Date Sampled: 12/20/98
Date Analyzed: 12/31/98
Dilution Factor: 1.0
I
I
I
I
Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane
127-18-4--------Tetrachloroethene --
108-88-3--------Toluene
-SEE CASE NARRATIVE. -
FORM I VOA
5.0
1. 0
1.0
1.0
1. 0
1.0
5.0
1.0
1.0
1.0
1.0
1. 0
0.1
1.0
1.0
1.0
1.0
1.0
1. 0
0.6
1. 0
1.0
2
1.0
1.0
1. 0
1.0
1.0
5.0
2.0
5.0
1.0
1.0
4
1.0
u u u u
u
U* u u
u u u u
J u
U*
u u u
u
J u u·
u u u u u
u u u u
u
u
u:T
i)J
J
00566
FORM 1 CLIENT SAMPLE NO.
1,,
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-22S
Lab Name: ECKENFELDER INC. Contract: EL PASO tab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V1215601
Matrix: (soil/water) WATER
,,ample wt/vol:
··Level: (low/med)
25.00 (g/mL) ML
LOW t Moisture: not dee.
·Ge Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812182-06
Lab File ID:
Date Sampled:
1218206
12/20/98
Date Analyzed: 12/31/98
Dilution Factor: 1.0
Soil Aliquot Volume: toil Extract Volume: ____ (uL)
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I ,,
I
0,
I
I
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
0.6 J
1.0 u
1.0 u
0.4 J
1.0 u
I
00578
FORM l CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
11
Lab Name: ECKENFELDER INC. Contract: EL PASO
W-22I
!lab ~ode: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
l\atrix: (soil/water) WATER Lab Sample ID: 9812182-07
,,ample I ,
evel:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
Lab File ID:
Date Sampled:
1218207D
12/20/98
,'1CMoisture: not dee.
~ Column: DB-624 ID: 0.53 (mm)
Date Analyzed: 01/01/99
Dilution Factor: 10.0 soil Extract Volume: ____ (uL) Soil Aliquot Volume:
I
I
I
I
I
I' v'
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2------c--Benzene
75-27-4---------Bromochloromethane /0
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-D~bromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,l-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,l-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene --78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane
127-18-4--------Tetrachloroethene --
108-88-3--------Toluene
= SEE CASE NARRATIVE.
FORM I VOA
Q
50 UD
%:-4 hID-
10 UD*
10 UD
10 UD
10 UD*
50 UD
10 UD
10 UD
10 UD
10 UD
0,8 JD
10 UD
10 UD
10 UD*
10 UD
10 UD
10 UD
10 UD
58 D
10 UD
20 D
140 D
0.4 JD
10 UD
10 UD
10 UD
10 UD so UD
cf O -4 .J-Bfl
so UD
10 UD
10 UD
110 D
10 UD
K: u
T u
u J rz
.J u J
.,,
:J
T
-J _;
--,)
00579
FORM 1 CLIENT SAMPLE NO. I
I
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-22I
Lab Name: ECKENFELDER INC. Contract: EL PASO
Batch No.: NA tab Code: NA
Matrix: (soil/water)
,gsample wt/vol:
SAS No.: NA SDG No.: FCX.Vl215601
/Level: (low/med)
WATER
25.00 (g/mL) ML
LOW
1% Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812182-07
Lab File ID: 1218207D
Date Sampled: 12/20/98
Date Analyzed: 01/01/99
Dilution Factor: 10.0
Soil Aliquot Volume: ,gsoil Extract Volume: ____ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
71-55-6---------1,1,l-Trichloroethane , 12 D
79-00-5---------1,1,2-Trichloroethane 10 UD
79-01-6---------Trichloroethene 10 D
75-01-4---------Vinyl chloride 3 JD
1330-20-7-------Xylene(total) 10 UD
FORM I VOA
I
-
I
00595
FORM 1 CLIENT SAMPLE.NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-AE
Lab Name: ECKENFELDER INC. Contract: EL PASO
Batch No. : NA tab Code: NA
Matrix: (soil/water)
fample wt/vol:
SAS No.: NA SDG No.: FCX.Vl215601
Level: (low/med)
,, Moisture: not dee.
WATER
25.00 (g/rnL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812182-08
Lab File ID: 1218208
Date Sampled: 12/19/98
Date Analyzed: 12/31/98
Dilution Factor: 1.0
,,oil Extract Volume: ____ (uL) Soil Aliquot Volume: ___ (uL)
I
I
I
I
I
I
I
I
D
u
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
67-64-1---------Acetone 5.0 u
71-43-2---------Benzene 1.0 u
75-27-4---------Bromochloromethane 1.0 u
75-27-4---------Bromodichloromethane 1.0 u
75-25-2---------Bromoforrn 1. 0 u
74-83-9---------Bromomethane 1.0 U*
78-93-3---------2-Butanone 5.0 u
75-15-0---------Carbon disull:iae 1.0 u
56-23-5---------Carbon tetrachloriae 1.0 u
108-90-7--------Chlorobenzene 1. 0 u
75-00-3---------Chloroethane 1.0 u
67-66-3---------Chloroform 1. 0 u
74-87-3---------Chloromethane 0.2 J
124-48-1--------Dibromochloromethane 1.0 u
96-12-8---------1,2-Dibromo-3-chloropropane 1. 0 U*
106-93-4--------1,2-Dibromoethane -1.0 u
95-50-1---------1,2-Dichlorobenzene 1.0 u
541-73-1--------1,3-Dichlorobenzene 1.0 u
106-46-7--------1,4-Dichlorobenzene 1.0 u
75-34-3---------1,1-Dichloroethane 1. 0 u
107-06-2--------1,2-Dichloroethane 1.0 u
75-35-4---------1,1-Dichloroethene 0.1 JB
156-59-2--------cis-l,2-Dichloroethene 1.0 u v:;
156-60-5--------trans-l,2-Dichloroethene 1.0 u
78-87-5---------1,2-Dichloropropane --1.0 u
10061-01-5------cis-l,3-Dichloropropene 1. 0 u
10061-02-6------trans-l,3-Dichloropropene 1.0 u
100-41-4--------Ethylbenzene --1.0 u
591-78-6--------2-Hexanone 5.0 u
75-09-2---------Methylene chioriae 2.0 u
108-10-1--------4-Methyl-2-pentanone 5.0 u
100-42-5--------Styrene 1.0 u
79-34-5---------1,1,2,2-Tetrachloroethane 1.0 u
127-18-4--------Tetrachloroethene --1.0 u
108-88-3--------Toluene 1. 0 u
= SEE CASE NARRATIVE.
FORM I VOA
I
I 00596
FORM 1 CLIENT SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-AE
Lab Name: ECKENFELDER INC. Contract: EL PASO
tab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
,a~pl~ wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Extract Volume: ____ (uL)
Lab Sample ID: 9812182-08
Lab File ID:
Date Sampled:
1218208
12/19/98
Date Analyzed: 12/31/98
Dilution Factor: 1.0
Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
R
D
u
I
I
I
I
I
I
I
I
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
I
I
I
00601
FORM l CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-lS
Lab Name: ECKENFELDER INC. Contract: EL PASO
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER Lab Sample ID: 9812182-09
lample wt/vol: 25. 00 (g/mL) ML Lab File ID: 1218209D
Level: (low/med) LOW I Moisture: not dee.
Date Sampled: 12/19/98
Date Analyzed: 12/22/98
Dilution Factor: 5.0
Soil Aliquot Volume:
GC Column: DB-624 ID: 0.53 (mm)
loil Extract Volume : ____ (uL)
CONCENTRATION UNITS:
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
67-64-1---------Acetone 25 UD
71-43-2---------Benzene 5.0 UD
75-27-4---------Bromochloromethane 5.0 UD
75-27-4---------Bromodichloromethane 5.0 UD
75-25-2---------Bromoform 5.0 UD
74-83-9---------Bromomethane 5.0 UD
78-93-3---------2-Butanone 25 UD
75-15-0---------Carbon disulfide 5.0 UD
56-23-5---------Carbon tetrachloride 0.6 JD
108-90-7--------Chlorobenzene 5.0 UD
75-00-3---------Chloroethane 5.0 UD
67-66-3---------Chloroform l JD
74-87-3---------Chloromethane 's.o :,A
124-48-1--------Dibromochloromethane 5.0 UD
96-12-8---------1,2-Dibromo-3-chloropropane_ 5.0 UD
106-93-4--------1,2-Dibromoethane 5.0 UD
95-50-1---------1,2-Dichlorobenzene 5.0 UD
541-73-1--------1,3-Dichlorobenzene 5.0 UD
106-46-7--------1,4-Dichlorobenzene 5.0 UD
75-34-3---------1,1-Dichloroethane 5.0 UD
107-06-2--------1,2-Dichloroethane 5.0 UD
75-35-4---------1,1-Dichloroethene ;;i..c~ -JI}
156-59-2--------cis-l,2-Dichloroethene 1.0 u
156-60-5--------trans-l,2-Dichloroethene 1. 0 u
78-87-5---------1,2-Dichloropropane --5.0 UD
10061-01-5------cis-l,3-Dichloropropene 5.0 UD
10061-02-6------trans-l,3-Dichloropropene 5.0 UD
100-41-4--------Ethylbenzene --5.0 UD
591-78-6--------2-Hexanone 25 UD
75-09-2---------Methylene chloride IC ·6-,--5 -
108-10-1--------4-Methyl-2-pentanone 25 UD
100-42-5--------Styrene 5.0 UD
79-34-5---------1,1,2,2-Tetrachloroethane 5.0 UD --127-18-4--------Tetrachloroethene /'-lo'"~ BE-O
108-88-3--------Toluene 5.0 UD
FORM I VOA
0
u
/J
(/
T
00602
FORM 1 CLIENT SAMPLE NO.
I
I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-lS
Name: ECKENFE.LDER INC. Contract: EL PASO Lab
ILab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER
lsample wt/vol: 25. 00 (g/mL) ML
Level: (low/med) LOW
.,. Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm) I soil Extract Volume : ____ (uL)
Lab Sample ID: 9812182-09
Lab File ID: 1218209D
Date Sampled: 12/19/98
Date Analyzed: 12/22/98
Dilution Factor: 5.0
Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
71-55-6~--------l,1,1-Trichloroethane 5.0 UD
79-00-5---------1,1,2-Trichloroethane 5.0 UD
79-01-6---------Trichloroethene 0.7 JD
75-01-4---------Vinyl chloride 5.0 UD
1330-20-7-------Xylene(total) 5.0 UD
FORM I VOA
I
I
I
FORM 1
00620
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-20S
Lab Name: ECKENFELDER INC. Contract: EL PASO
[lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water)
lample wt/vol:
Level: (low/med) I Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812182-10
Lab File ID: 1218210
Date Sampled: 12/20/98
Date Analyzed: 12/31/98
Dilution Factor: 1.0
loil Extract Volume: ____ (uL) Soil Aliquot Volume: ---'--(UL)
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone 5.0
71-43-2---------Benzene 1.0
75-27-4---------Bromochloromethane 1.0
75-27-4---------Bromodichloromethane 1.0
75-25-2---------Bromoform 1.0
74-83-9---------Bromomethane 1.0
78-93-3---------2-Butanone 5.0
75-15-0---------Carbon disulb.de 1.0
56-23-5---------Carbon tetrachlon.de 0.1
108-90-7--------Chlorobenzene 1.0
75-00-3---------Chloroethane 1.0
67-66-3---------Chloroform 0.2
74-87-3---------Chloromethane 1.0
124-48-1--------Dibromochloromethane 1.0
96-12-8---------1,2-Dibromo-3-chloropropane_ 1.0
106-93-4--------1,2-Dibromoethane 1. 0
95-50-1---------1,2-Dichlorobenzene 1. 0
541-73-1--------1,3-Dichlorobenzene 1.0
106-46-7--------1,4-Dichlorobenzene 1.0
75-34-3---------1,1-Dichloroethane 1.0
107-06-2--------1,2-Dichloroethane 1.0
75-35-4---------1,1-Dichloroethene I . 0 -0--ri,
156-59-2--------cis-l,2-Dichloroethene 4
156-60-5--------trans-l,2-Dichloroethene --1.0
78-87-5---------1,2-Dichloropropane 0.4
10061-01-5------cis-l,3-Dichloropropene 1.0
10061-02-6------trans-l,3-Dichloropropene __ 1.0
100-41-4--------Ethylbenzene 1.0
591-78-6--------2-Hexanone 5.0
75-09-2---------Methylene chloride ,) , C ,lr.-4
108-10-1--------4-Methyl-2-pentanone 5.0
100-42-5--------styrene 1.0
79-34-5---------1,1,2,2-Tetrachloroethane 1.0
127-18-4--------Tetrachloroethene --J---, -3--fi.
108-88-3--------Toluene 1.0
*=SEE CASE NARRATIVE.
FORM I VOA
Q
u u u
u u
U*
u
u
J u
u
J u
u
U* u u
u u u u
JB
u
J u u u u
-if-
u u u
e-!)
u
VT
J ))_'
J
,z
I ~ I
J
V J
T
.J
V
V
----.)
00621
FORM l CLIENT SAMPLE NO.
I
I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-20S
Name: ECKENFELDER INC. Contract: EL PASO Lab
ILab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl21560l
IMatrix: (soil/water)
Sample wt/vol:
•
Level: (low/med)
% Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
lsoil Extract Volume : ____ (uL)
Lab Sample ID: 9812182-10
Lab File ID: 1218210
Date Sampled: 12/20/98
Date Analyzed: 12/31/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
•
I
I
D
I
I
I
71-55-6--

-

-

-

-

-

-
-1, 1, 1-Trichlo·roethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
1. 0 u
1. 0 u
l
1.0 u
1.0 u
I
I
I
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ECKENFELDER INC. Contract: EL PASO
00646
CLIENT SAMPLE NO.
TRIP BLA
NK #1202
Jab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vl215601
Matrix: (soil/water) WATER Lab Sample ID: 9812182-11
lample wt/vol: 25.00 (g/mL) ML Lab File ID: 1218211
Level: (low/med) LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
loil Extract Volume: ____ (uL)
Date Sampled: 12/20/98
Date Analyzed: 12/31/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulb.de
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
--
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane
127-18-4--------Tetrachloroethene --
108-88-3--------Toluene
= SEE CASE NARRATIVE.
FORM I VOA
5.0 u
0.06 JB
1.0 U·
1. 0 u
1.0 u
1. 0 U*
5.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 U*
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1. 0 u
0.1 JB
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1. 0 u
5.0 u
0.5 J
5.0 u
1.0 u
1.0 u
1.0 u
1.0 u
f.l...
UJ
UT
I 1
' uT
VJ
uT
T Uj
I
I 00647
FORM 1 CLIENT SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ECKENFELDER INC. Contract: EL PASO
TRIP BLA
NK #1202
lab Code: NA Batch No. : NA SAS No.: NA SDG No. : FCX .Vl215601
Matrix: (soil/water) WATER
fample wt/vol:
Level: (low/med) I Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
foil Extract Volume: ____ (uL)
Lab Sample ID: 9812182-11
Lab File ID: 1218211
Date Sampled: 12/20/98
Date Analyzed: 12/31/98
Dilution Factor: 1.0
Soil Aliquot Volume: ___ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
71-55-6---------1,1,1-Trichloroethane 1.0 u
79-00-5---------1,1,2-Trichloroethane 1. 0 u
79-01-6---------Trichloroethene 1. 0 u
75-01-4---------Vinyl chloride 1.0 u
1330-20-7-------Xylene(total) 1.0 u
FORM I VOA
I
I FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
ECKENFELDER INC. Contract: EL PASO
00654
CLIENT SAMPLE NO.
HOLDING
BLANK 122298
j,ab ~ode: NA Batch No.: NA
~atrix: (soil/water) WATER
SAS No.: NA SDG No.: FCX.Vl215601
Lab Sample ID: 9812182-12
t,ample
~evel:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
Lab File ID:
Date Sampled:
1218212
12/22/98
1-CMoisture: not dee.
~ Column: DB-624 ID: 0.53 (mm)
Date Analyzed: 12/31/98
Dilution Factor: 1.0
I
I
I
I
I
I
I
I
I
I
I
I
Extract Volume: ____ (uL) Soil Aliquot Volume:
*
CAS NO. COMPOUND
67-64-1---------Acetone
71-43-2---------Benzene
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulriae
56-23-5---------Carbon tetrachloriae
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chloriae
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane
127-18-4--------Tetrachloroethene --
108-88-3--------Toluene
SEE CASE NARRATIVE.
FORM I VOA
5.0
1.0
1.0
1.0
1. 0
1. 0
5.0
1.0
1. 0
1. 0
1.0
1.0
1.0
1.0
1. 0
1.0
1.0
1.0
1.0
1.0
1.0
1. 0
1.0
1.0
1. 0
1.0
1.0
1.0
5.0
2.0
5.0
1. 0
1.0
1.0
1.0
____ (uL)
:, ,q~ r-11 9~.i Q
u u
U*
u u
U*
u
u u u
u
u u u
U*
u u u
u u u u u
u u u u
u u u
u u
,U
u u
l?...
i)
kl
uT
u J
v' .J
J VJ
I
I FORM 1
00655
CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: ECKENFELDER INC. Contract: EL PASO
HOLDING
BLANK 122298
[
b Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vl215601
atrix: (soil/water) WATER
.,mple
'f!evel:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
'C
Moisture: not dee.
Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9812182-12
Lab File ID:
Date Sampled:
1218212
12/22/98
Date Analyzed: 12/31/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL) .oil Extract Volume: ____ (uL)
CONCENTRATION UNITS:
I
I
I
I
I
I
I
I
I
I
I
I
'CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
71-55-6---------1,1,1-Trichloroethane 1. 0 u
79-00-5---------1,1,2-Trichlo'roethane 1.0 u
79-01-6---------Trichloroethene 1.0 u
75-01-4---------Vinyl chloride 1.0 u
1330-20-7-------Xylene(total) 1.0 u
FORM I VOA
I
I
U.S. EPA -CLP
l
INORGANIC ANALYSIS DATA SHEET
00039
EPA SAMPLE NO. I
I Name: I W-31s
~E~C~K~E~N~F~E~L~D~E~R.:....;I~N~C::..:...· __________ Contract:_:E~lc...::P~a~s~o:.....:E~n~e~r~g~y!....l ___________ _J
Lab Code: Case No.: _______ _ SAS No.: _______ _
frix (soil/water): ~w~a~t~e~r'---
Level (low/med):
folids: 0.0
Lab Sample ID: 9811157-01 ---'-='--'--~'---
Date Received: ___ l_l_/_2_0~/_9_8 __
SDG No.: 98P03(icp)
98P06 (Hg)
I Concentration Units {ug/L or mg/kg dry weight) : ___ ~u~g~/~L'---
I
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
,7440-39-3
[7440-41-7
17440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before:
Analyte
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
:Cabal t
Copper
Iron
Lead
Magnesium
Manganese
!Mercury
:Nickel ' jPotassium
Selenium
Silver
Sodium
Thallium
!Vanadium
]Zinc
:cyanide
----Iler After:
Comments:
I
I
i
'
' Concentration C Q M
10800 : p
1.2 u ' p ' 1.3 u ' p ' 113 B ' p ' 0.32 B : p
0.10 u ' p ' 11700 ' p ' 22.2 : p
7.1 B ' p ' 10.6 B ' p ' ' 12800 ' p ' ' ' 4.0 : p ' ' 6010 : p ' ' 97 5 ' p ' ' ' 0.10 ' u : CV: ' 11. 8 B : p:
3390 B E : Pi
4. 9 B N ' Pi ' 0.10 ' u ' p:
7410 : E ' pl
1. 4 u
28.0 B
21. 9
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
I
I
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
00040
EPA SAMPLE NO.
W-31s Dupe lb Name: ECKENFELDER INC. Contract: El Paso E,nergy I ====='-'-'------------------~~---------~
Lab Code: Case No.: SAS No.: ----------------ltrix (soil/water): _w_a_t_e_r __ _ Lab Sample ID: 9811157-02 --'-=='--'-'--
Level (low/med): Date Received: 11/20/98 ___ ;._ ___ _
I solids: o.o
SDG No.: 98P03(icp)
98P06 (Hg)
I
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight): ug/L ---~----
I ' ' CAS Analyte Concentration C ' Q M ' No. ' ' : ' ' ' ' ' ' 7429-90-5 Aluminum 4 9800 : p :
7440-36-0 Antimony 1.8 u ' p ' ' ' 7440-38-2 Arsenic l. 3 u : p ' ' 7440-39-3 Barium 397 ' p ' 7440-41-7 Beryllium 2.0 B ' p ' 7440-43-9 Cadmium 0.29 B ' p ' 7440-70-2 Calcium 17600 ' p ' 17440-47-3 Chromium 118 ' I p ' !7440-48-4 Cobalt 25.5 B ' : p ' ' ' ' 17440-50-8 Copper I 48.6 ' ' p
!7439-89-6 Iron ' 64100 ' I p ' ' ' ' ' ' ' 17439-92-1 Lead : 13.9 ' ' ' p ' '
I
' ' ' ' 17439-95-4 Magnesium ' 17400 ' I ' p ' ' ' ' ' ' ' !7439-96-5 Manganese ' 1610 ' ' ' p ' 7439-97-6 Mercury ' 0.10 ' u ' : cv: ' ' !
7440-02-0 Nickel ' 50.3 ' ' ' p ' ' ' '
I
,r 7440-09-7 Potassium ' 12600 ' ' E ' p ' ' ! ' ,7782-49-2 Selenium ' 3.2 ' B ' N ' p
' !
:7440-22-4 Silver ' 0.50 : u : I p
' :7440-23-5 ' Sodium ' 8330 i i E ' p ,f
l7440-28-0 Thallium ' l. 4 i u ; ' p
!7440-62-2 Vanadium ' 131 : : ' p ' !7440-66-6 Zinc ' 116 I I : p ' ' Cyanide i i i ' ' :
I ' i ; ' ' I
Color Before: Clarity Before: Texture: ----lolor After: Clarity After: Artifacts:
Comments: •---------
FORM I -IN
I
I
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
00041
EPA SAMPLE NO.
EB @ W-31i t Name: ECKENFELDER INC. Contract: El Paso Energy I =====:..:_=;:_c___________ -"---"--'"-'-'-'-''-'--'-· ------------'
Lab Code: Case No.: _______ _ SAS No.: --------ltrix {soil/water): ~w~a~t~e~r:_ __
Level {low/med):
lsolids: o.o
Lab Sample ID: _ _:_98~1~1~1~5~7~-~0~3:__
Date Received: 11/20/98 --=c..=..:..:...c:...c... __
I Concentration Units {ug/L or mg/kg dry weight): ug/L
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
Analyte
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
7440-09-7 Potassium
I
I
I
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before:
Selenium
:Silver
;sodium
!Thallium
:vanadium
\Zinc
:cyanide
'
----liar After:
Comments:
I
I
f
Concentration C Q
7.0 u
l. 2 u
l. 7 u
0.24 B
0.10 u
0.12 B
626 B
0.30 u
0.25 B
0. 4 5 B
5. 7 u
0.80 u
19.B u
0.32 B
0.10 u
0.63 B
16 0 B E
' 3.1 : B : N
' 0.10 i u '
' 918 ; B ' E
' l. 4 ' u ' 0.29 B ' 0.84 B
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
SDG No.: 98P03{icp)
98P06 {Hg).
M
p
p
p
p
p
p
p
p
p
p
p
p
p
p ' : CV [
p
' ' p ' '
' Pi
' p, .:r
' p ;
' pl
' p,
' '
! !
I
I
U.S. EPA -CLP
l I INORGANIC ANALYSIS DATA SHEET
lb Name: ECKENFELDER INC. Contract: El Paso Energy
Lab Code: _____ Case No. : _______ _ SAS No. : _______ _ ltrix {soil/water): _w_a_t_e_r __ _ Lab Sample ID: 9811157-04
Level {low/med): Date Received: 11/20/98 I Solids: o.o
I Concentration Units {ug/L or mg/kg dry weight) =---~u~g~/~L:.._ __
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
' ' !Analyte
' :
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
:calcium
!chromium
!cobalt
!copper
!rron ' :Lead ' !Magnesium
:Manganese
Mercury
Nickel
7440-09-7 Potassium
7782-49-2 Selenium
7440-22-4 Silver
7440-23-5 Sodium
7440-28-0 Thallium
7440-62-2 Vanadium
7440-66-6 Zinc
' ' ' ' ' ' ' ' :
' ' Concentration ' C Q ' ' ' :
74.0 ' B ' l. 4 u ' ' l. 3 u ' ' 27.l B :
0.10 u :
0.10 u ' ' 8570
l. 2 B
0.58 B
0.80 u
39.9 B
l. 7 B
2800 B
4.5 B
0.10 u
1.8 B
2 610 B E
4.8 B N
0.17 B
5350 E
4.0 u
l. 0 B
37. 5
00042
EPA SAMPLE NO.
' :
' :
W-3li
SDG No.: 98P03{icp)
98P06 {Hg)·
M
p :
p ' ' p ' ' p ' ' p ' ' p ' ' p
p
p
p
p
p
p
p
cv:
p
p ,-' .J
p
p
p ,f
p
p ' P!
' ' >-----~Cyanide :~•--------f----+---------1--: I
Color Before: Clarity Before: Texture: ----lolor After: Clarity After: Artifacts:
Comments: ,---------
FORM I -IN
U.S. EPA -CLP
l
00043
EPA SAMPLE NO.
I
I
I INORGANIC ANALYSIS DATA SHEET
I ~-32i t Name: ECKENFELDER INC. Contract:__:E~l:......:P~a~s~o:......:E~n~e~r~g~y'-'-------------'
Lab Code: _____ Case No. : _______ _ SAS No.: _______ _
ltrix (soil/water I: _w~a_t_e~r'----
Level (low/med):
lsolids: o.o
Lab· Sample ID: 9811174-01 ----'---'---
Date Received: __ ~l~l~/~2~1~/~9~8'---
I
I
I
I
I
Concentration Units {ug/L or mg/kg dry weight) : ___ ~u~g~/~L:.._ __
I
I
I
I
' CAS No. Analyte
7429-90-5 :Aluminum
7440-36-0 !Antimony
7440-38-2 \Arsenic
7440-39-3 !Barium
7440-41-7 !Beryllium
7440-43-9 !cadmium
-: ,7440-70 2 Calcium
:7440-47-3
:7440-48-4
!7440-50-8
:7439-89-6 17439-92-l
7439-95-4
7439-96-5
7439-97-6 1Mercury
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
!Nickel ,7440-02-0 ' 17440-09-7 \Potassium ' !7782-49-2 !Selenium
7440-22-4 !Silver
7440-23-5 !Sodium
7440-28-0 !Thallium
7440-62-2 !Vanadium
7440-66-6 !Zinc
' ;cyanide ' ' l
Color Before: ----lalor After:
Comments:
I
' '
' ' Concentration C ' Q ' ' ' ' ' 1200 :
1. 2 u :
1. 3 u ' ' 10.2 B ' ' 0.10 u :
0.10 u ' ' 16300 '
11. l
1. 3 B
3.3 B
1200
1. 7 B
5480
28.8
0 10 u ' 7.0 B ' ' ' 17 30 B ' E ' ' 4.0 B ' N ' 0.10 u ' 5920 ' E
1. 5 B ' ' 7.1 B ' ' 244 !
'
l l
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
'
'
'
'
'
'
SDG No.: 98P03(icp)
98P06 (Hg)·
M
p
p
p
p
p
p
p
p
p
p
p
p
p
p
cv' ' p ' ' p ' ' .r
p :.
P!
p : . .T
p
p
p
'
'
I
I
I U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
I Name: ~E~C~KE_::::N~F:..:::E~L~D~E~R:....:I~N~C::..:_. ___________ contract: El Paso Energy
Lab Code: Case No. : _______ _ SAS No. : _______ _
ltrix (soil/water): ~w~a~t~e~r=----
Level (low/med):
lsolids: 0.0
Lab Sample ID: 9811174-02
Date Received: ___ 1_1_/_2_1_/_9_8 __
I ug/L Concentration Units (ug/L or mg/kg dry weight): ___ ....::.=-=----
I CAS No.
7429-90-5
I 7440-36-0
7440-38-2
7440-39-3
I ,7440-41-7
17440-43-9
i7440-70-2
]7440-47-3
I !7440-48-4
7440-50-8
7439-89-6
7439-92-1
I 7439-95-4
,7439-96-5 ' :7439-97-6
:7440-02-0 ' I :7440-09-7
h1a2-49-2 ' :7440-22-4 ' !7440-23-5
I !7 4 4 0-28-0
i7440-62-2
!7440-66-6
' '
I
Color Before: llor After:
Comments: I
I
f
Analyte
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Cyanide
Concentration. C Q
6.0 u
l. 2 u
l. 3 u
47.2 B
0.10 u
0.10 u
4200 B
0.30 u
0.54 B
12.6 B
12.8 B
2.4 B
2440 B
3 4 B
0.10 u ' 2.4 B :
1480 B ' E ' ' C 2.0 B ' N ' 0.17 ' B ' ' 4440 ' B ; E
l. 4 ' u ;
0.20 u
8. 9 B
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
00044
EPA SAMPLE NO.
Wooten Well
SDG No.: 98P03(icp)
98P06 (Hg)·
jl:51'! ~-;7·9'1 ,,..
M
p
p
p
p
p
p
p
p
p
p
p
p
p
p
: CV
' p ' ' : p
' P, '
' p :
' p;
! p ' ' p
p
00045
I
I
I U.S. EPA -CLP
1 EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
lab Name: ECKENFELDER INC.
Hinson Well
Contract: El Paso Energy
Lab Code: _____ Case No. : _______ _
llatrix (soil/water): _w~a~t~e~r __ _
SAS No.: _______ _ SDG No.: 98P03(icp)
98P06 (Hg)
Lab Sample ID: 9811174-03
Level (low/med): Date Received: --~1~1~/~2~1~/~9~8:__ I Solids:
I
I
I
I
I
I
I
I
I
0.0
Concentration Units (ug/L or mg/kg dry weight): ug/L -----"-~---
' ' ' ' CAS No. Analyte Concentration C ' Q ' M ' ' i ' i7429-90-5 Aluminum 3.5 u ' p ' !7440-36-0 Antimony 1. 6 u ' p ' ' :7440-38-2 Arsenic 1. 3 u p ' ' !7440-39-3 Barium 12.5 B p ' ' i --' ,7440 41 7 Beryllium 0.10 U P ! 7 4 4 0-4 3-9 Cadmium .---~0-. ~1~0--------C,U--.--------'-'p,....;
:7440-70-2 Calcium 25600 P
:7440-47-3 Chromium 0.30 U P
:7440-48-4 Cobalt 0.36 B P
:7440-50-8 Copper O. 78 B P
:7439-89-6 Iron 110 P
:7439-92-1 Lead o. 80 u P
:7439-95-4 Magnesium 5270 P
:7439-96-5 Manganese 7 O B P
!7439-97-6 Mercury
:7440-02-0 Nickel
17440-09-7 Potassium
h782-49-2 Selenium
h440-22-4 Silver
h440-23-5 Sodium
7440-28-0 Thallium
7440-62-2 Vanadium
7440-66-6 Zinc
0.10 u ' 1 CV:
Cyanide 1------l
'
0. 7 9
905
1. 4
0.10
10300
1.4
0.20
8.2
B Pi
B E p i
u N p !
u ' Pi
' E ' Pj
u p .
u p
B p
Color Before: Clarity Before: Texture: ----lalor After: Clarity After: Artifacts:
Comn1ents:
I
FORM I -IN
.r
I
I
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
00046
EPA SAMPLE NO.
lb Name: I W-20I
=E~C~KE=N~F=E~L~D~E~R:....:I~N~C~·:_ __________ contract: -=E=l:....:P~a~•~o:....:E~n~e~r~g~yC.J. ___________ ..J
Lab Code: Case No.: _______ _ SAS No.: _______ _ SDG No.: 98P04(icp)
ltrix (soil/water): _w~a~t~e~r __ _ Lab Sample ID: 9812156-01 --------------
Level (low/med): Date Received: --=1=2~/=1~7~/~9~8 __ I solids: 0.0
\
Concentration Units (ug/L or mg/kg dry weight): ug/L ---==---I
I
I
[',Li,.,, ,;, Cf f
~--~----,------,---~------.--,-1'-:, ,J : ! : r
I
I
I
I
I
I
!CAS No. :Analyte Concentration C Q M !
: t I
1 l :
74.5 B p
' '
:7429-90-5 :Aluminum
:7440-36-0 :Antimony
7440-38-2 Arsenic
7440-39-3 Barium
7440-41-7 Beryllium
17440-43-9 :cadmium
!7440-70-2 Calcium
!7440-47-3 Chromium
'7440-48-4 Cobalt
7440-50-8 Copper
7439-89-6 Iron
7439-92-1 Lead
7439-95-4 Magnesium
h439-96-5 Manganese
h439-97-6 Mercury
17440-02-0 :Nickel
h440-09-7 :Potassium
'. '
1. 3 B p
' ' :7782-4 9-2 !Selenium ' : ' 7 ' ' !7440-22-4 \Silver ' :
17440-23-5 !Sodium ' ' ' ' 7440-28-0 !Thallium ' ' !
7440-62-2 !Vanadium ' ' 7440-66-6 JZinc ! ' !Cyanide ' ! '
' ' ! ' '
Color Before: Clarity Before: Texture: ----l,1or After: Clarity After: Artifacts:
Comments:
I
FORM I -IN
I
I
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
00047
EPA SAMPLE NO.
I Name: I W-31I
_E_C_K_E_N_F_E_L_D_E_R_I_N_C_. ___________ Contract:_;:E~l'--'P~a_s~o'--'E~n~e~r_g~y'-'------------'
Lab Code: Case No.: --------SAS No.: --------SDG No.: 98P04(icp)
lrix (soil/water): _w_a_t_e_r __ _ Lab Sample ID: --------9812156-02
Level (low/med): Date Received: 12/17/98 __ ...c.._.c..;:._;_.c....c.. __
lsolids: 0.0
I Concentration Units (ug/L or mg/kg dry weight): ug/L , tu ✓l-1~/-rf
I ' ' ,r
' ' ' :cAS No. !Analyte Concentration C Q M ' ' ; ' ' ' l l
I 7429-90-5 :Aluminum
7440-36-0 !Antimony
7440-38-2 \Arsenic
7440-39-3 !Barium
7440-41-7 \Beryllium I 7440-43-9 :cadmium
7440-70-2 !calcium
:7440-47-3 Chromium
I !7440-48-4 Cobalt
[7440-50-0 Copper
' 17439-89-6 Iron 20.8 B p
:7439-92-1 Lead
I 17439-95-4 Magnesium
llo9-96-5 Manganese 4.8 B p
' l7439-97-6 ,Mercury
7440-02-0 !Nickel
I 7440-09-7 !Potassium
7782-49-2 /Selenium
7440-22-4 iSilver
7440-23-5 !Sodium ' '
I I
I )7440-28-0 !Thallium
I I
!7440-62-2 !Vanadium
17440-66-6 1Zinc ! :cyanide
I ' ' ' '
Color Before: Clarity Before: Texture:
lolor After: Clarity After: Artifacts:
Comments:
I
I
11 FORM I -IN
I
I
I
lb Name:
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
ECKENFELDER INC. Contract: El Paso Energy ====="--'=::__ _________ _
00048
EPA SAMPLE NO.
W-12 I
Lab Code: _____ Case No. : _______ _ SAS No.: _______ _ SDG No.: 98P04(icp) ltrix (soil/water): _w_a_t_e_r __ _
Level (low/med): I solids: o.o
Lab Sample ID: _ __:.9~8~1~2~15:..:.6-_0~3::___
Date Received: --~1~2~/~1~7~/~9~8:.__
I
I
Concentration Units (ug/L or mg/kg dry weight): ---~u~g~/~L:._ __
I
I
I
I
I
I
I
CAS No. Analyte
7429-90-5 Aluminum
7440-36-0 Antimony
,7440-38-2 Arsenic
!7440-39-3 Barium
!7440-41-7 Beryllium
7440-43-9 Cadmium
7440-70-2 Calcium
7440-47-3 Chromium
7440-48-4 Cobalt
7440-50-8 Copper
7439-89-6 Iron
!7439-92-1 Lead ' ]7439-95-4 Magnesium
' ,7439-96-5 :Manganese
h439-97-6 !Mercury
h440-02-0 !Nickel
!7440-09-7 lPotassium
7782-49-2 !Selenium
7440-22-4 !Silver
7440-23-5 :sodium ' 7440-28-0 !Thallium
7440-62-2 \vanadium
7440-66-6 !Zinc
!cyanide
' !
Color Before:
f,1or After:
Comments:
' ' Concentration C Q ' \ ' ' ' ' ' ' ' ' ' ' ' ' ' \ \
' ' ' ' ' ' ' ' 21. 3 ' B ' ' ' ' \ ' ' ' ' ' ' ' ' ' 4 • 1 ' B '
i
'
' ' i ! ' T i '
' i
' '
' ' !
Clarity Before: Texture:
Clarity After: Artifacts:
M
' ' \
\
' ' ' ' ' ' p ' ' ' !
' ' P,
' !
'
'
'
!
'
1---------
FORM I -IN
I
I
U.S. EPA -CLP
1 I INORGANIC ANALYSIS DATA SHEET
I Name: ECKENFELDER INC. Contract: El Paso Energy
Lab Code: Case No.: _______ _ SAS No.: _______ _
tlrix I soil/water I : .;.w..:a:..:t:..:e..:rc_ __
Level (low/med):
lsolids: 0.0
Lab Sample ID: 9812156-04 _....:..;:..::.=..:.:......:..:__
Date Received: 12/17 /98 ---'--'--'---
00049
EPA SAMPLE NO.
W-31 s
SDG No.: 98P04(icp)
I
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight) : ___ :..:u~g~/:..:L=----
I
I
I
Color
Iller
I
lf
CAS No. Analyte
7429-90-5 Aluminum
7440-36-0 Antimony
17440-38-2 Arsenic
!7440-39-3 Barium
Beryllium !7440-41-7
:7440-43-9 :cadmium
17440-70-2 Calcium
[7440-47-3
17440-48-4
:7440-50-8
:7439-89-6
17439-92-1
!7439-95-4
:7439-96-5
h439-97-6
]7440-02-0
!7440-09-7
!7782-49-2
l7440-22-4
17440-23-5
h440-2e-o h44 □-62-2
!]440-66-6 :
Before:
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Cyanide
----
After:
' ' i ' ' : Concentration C : Q M
! ' ' ' ' ' ' ' ' ' : ' ' ' ' ' ' : ' ' ' . ' ' ' ' ' ' ' : ' '
4730 p
1420 p
!
' !
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
I
I
I U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
00050
EPA SAMPLE NO.
W-AA lb Name: ECKENFELDER INC. Contract: El Paso Energy I -=-==::....:-=..::.c..::c.......c.....c..___________ -------~~------------~
Case No.: --------SAS No.: _______ _
tr1x (soil/water): water I~ ~ode:
-----Lab Sample ID: _ _.:9~8~1~2~1~5~6~--0~5:;...._
Ivel I low/med) :
Solids: 0.0
Date Received: 12/17/98 ---'----'-'-'---
I
I
I
Concentration Units (ug/L or mg/kg dry weight) =---~u~g~/~L:;_ __
I
I
I
I
1·
I
rj',lor
ll1or
0
I
CAS No. Analyte
7429-90-5 Aluminum
7440-36-0 Antimony
7440-38-2 Arsenic
7440-39-3 Barium
7440-41-7
,7440-43-9
!7440-70-2
!7440-47-3
!7440-48-4
:7440-50-8
0 7439-89-6
7439-92-1
7439-95-4
,7439-96-5
:7439-97-6
h 4 40-02-0
17440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
:7440-62-2
:7440-66-6
' '
'
Before:
After:
:Beryllium
!cadmium
!calcium
!chromium
!cobalt
' :copper
!rron
!Lead ' JMagnesium
tManganese
!Mercury
!Nickel
[ Potassi urn
!Selenium
]Silver
\Sodium
tThallium
!vanadium
iZinc
!Cyanide
l
Concentration C Q
4380
1420
' ' ;
' l
' l
' ;
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
SDG No.: 98P04(icp)
M
p
p
'
'
'
'
I
I
I U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
LI Name: ECKENFELDER INC. Contract: El Paso Energy ====="---==-----------
Li Code: Case No.: -------SAS No. : _______ _ -rix (soil/water): 0w~a~t~e~r=---Lab Sample ID: _ _.:9~8~1~2~1~5~6~--0~6=--
I.el (low/med):
olids:
I
0.0
Date Received: 12/17/98 ----'---'--'--'---
00051
EPA SAMPLE NO.
W-AB
SDG No.: 98P04(icp)
Concentration Units (ug/L or mg/kg dry weight) : ___ ~u~g~/~L:._ __
' ' !CAS No.
' :
:
!Analyte : '
Concentration C Q M I
I
I
:7429-90-5 :Aluminum
17440-36-0 lAntimony
!7440-38-2 !Arsenic
\7440-39-3 \Barium
!7440-41-7 Beryllium ! 7 4 4 0-4 3-9 Cadmium .---------l-----:--------!--:
I
D , ..
I
:7440-70-2 Calcium
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
17439-96-5
!7439-97-6
17440-02-0
!J440-09-7
17782-49-2
!74 4 0-22-4
!7440-23-s 17440-28-0
7440-62-2
7440-66-6
Chromium
Cobalt
Copper
!Iron ' :Lead ' !Magnesium
:Manganese
:Mercury
!Nickel
'Potassium
Selenium
Silver
,Sodium
[Thallium
!V~nadium
:Zinc
!Cyanide I-------<
if.lor Before:
1l1ar After:
I ,,
----
'
' :
6 7
0.10
Clarity Before:
Clarity After:
FORM I -IN
' ' ' ' ' ' :
' ' ' '
'
'
' ' '
' !
'
B p
' ' u ' p ' ' ' ' ' ' ' ' ' T
Texture:
Artifacts:
'
'
I
U.S. EPA -CLP
1
I
I INORGANIC ANALYSIS DATA SHEET
lb Name: ECKENFELDER INC. Contract: El Paso Energy
Lab Code: Case No.: _______ _ SAS No.: _______ _
f.trix (soil/water
.Level (low/med): I Solids:
I
) : water
0.0
Lab Sample ID: 9812163-01 _....c..c..c...c..:;_:..::.......:..;:..__
Date Received: ___ 1_2_/_1_8_/_9_8 __
Concentration Units (ug/L or mg/kg dry weight): ug/L ---==---
I
I
I
I
IC,olor
olor
I
CAS No.
:
!Analyte
!
7429-90-5 :Aluminum
7440-36-0 !Antimony
7440-38-2 Arsenic
:7440-39-3 Barium
!7440-41-7 Beryllium
!7440-43-9 :cadmium
7440-70-2 !calcium
7440-47-3 !chromium
7440-48-4 !cobalt
7440-50-8 'copper
7439-89-6 Iron
7439-92-1 Lead
7439-95-4 Magnesium
7439-96-5 Manganese
7439-97-6 Mercury
7440-02-0 Nickel
h44o-os-7 Potassium
7782-49-2 Selenium
7!40-22-4 Silver
7440-23-5 :Sodium
!7440-28-0 iThallium
:7440-62-2 !Vanadium
i7440-66-6 !Zinc
' :cyanide '
l '
Before: ----
After:
Concentration C Q
13400
1580 ' ' 15.0
' I
' '
'
'
l
' l
' :
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
00052
EPA SAMPLE NO.
AA121798
SDG No.: 98P04 (icp)
98P08(Hg)
' /Ji-ff
M
p
p
. CV
' ' '
' ' !
' '
l
' !
l l
00053 I
I U.S. EPA -CLP
1 EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
t Name: ECKENFELDER INC. Contract: El Paso Energy
Lab Code: _____ Case No. : _______ _ SAS No.: _______ _
Jrix (soil/water ) : water Lab Sample ID: _ _:_9~8~1~2~1~63~--0~2:..__
Level (low/med): Date· Received: __ ..:l..:2:.:./..:l:..:8:.:./~9"8'---
lsolids: ~o:..;·~o ___ _
Concentration Units {ug/L or mg/kg dry weight) : ___ ..:u~g~/-=L=----
0
I
I
I
' ' CAS No. jAnalyte
:
7429-90-5 Aluminum
7440-36-0 Antimony
7440-38-2 Arsenic
7440-39-3 Barium
7440-41-7 Beryllium
7440-43-9 Cadmium
7440-70-2 Calcium
7440-47-3 ,Chromium
7440-48-4 ' 'Cobalt
7440-50-8 Copper
7439-89-6 Iron
7439-92-1 Lead
7439-95-4 :Magnesium
7439-96-5 !Manganese
7439-97-6 :Mercury
7440-02-0 !Nickel
7440-09-7 [Potassium
7782-49-2 !Selenium
7440-22-4 1Silver
7440-23-5 !Sodium
7440-28-0 !Thallium
7440-62-2 \vanadium
7440-66-6 !Zinc
:cyanide
' '
Color Before: ___ _ llor After:
Comments:
T ' ' Concentration C Q
'
3920
171 .
' ' ' ' ' ' ! T ' :
!
'
Clarity Before: Texture:
Clarity After: Artifacts:
W-24 s
SDG No.: 98P04 (icp)
:
M ' ' ' ' ' ' ' ' '
p
p
.
!
' ! :
!
,_, --------
FORM I -IN
I
I
1. ..
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
t Name: ~E~C~KE,:,:N~F~E~L~D~E~Rc....;I~N~C::..:.· __________ Contract: El Paso Energy
Lab Code: Case No.: _______ _
Btrix (soil/water): ~w~a~t~e~r __ _
SAS No.: ________ _
Lab Sample ID: 9812163-03 ---'-=....:..:..::.......:..;__
Level (low/med): Date Received: ___ 1_2_/_1_8~/_9_8 __ I solids: 0.0
00054
EPA SAMPLE NO.
W-5 s
SDG No.: 98P04(icp)
98P07 (Hg)
Concentration Units (ug/L or mg/kg dry weight) =---~u~g~/~L:;_ __ _
' ' !CAS No.
'
I 17429-90-5
!7440-36-0
!7440-38-2
!7440-39-3
!7440-41-7
\7440-43-9
!7440-70-2
:7440-47-3
I :7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
17440-02-0
I 17440-09-7
h7a2-4 9-2 ' 17440-22-4 ' ]7440-23-5
!7440-28-0
!7440-62-2
!7440-66-6
I
Color Before: l1or After:
.fmments:
I
f
Analyte
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
!copper ' 1Iron
Lead
Magnesium
Manganese
Mercury
:Nickel ' :Potassium
!selenium
JSilver
:sodium
!Thallium
]Vanadium
!Zinc
:cyanide
' ' ' Concentration C Q M I ' ' ' ' ' I I
I ' ' ' ' ' I
' ' ' ' ' ' ' '
11100 p
1430 p
10.2 : CV
'
'
i : 7
: ' '
! :
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
D
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
00055
EPA SAMPLE NO.
t Name: I W-8 i
;E~C~KE=N~F;E~L~D~E~R:.....:I~N~C::..:...· __________ contract:-=E~lc_;;P~a~s~o:.....:E~n~e~r~g~yc..J. ___________ _,
Lab Code: -----Case No.:--------SAS No.: --------ftrix (soil/water): ~w~a~t~e~r:..._ __ Lab Sample ID: 9812163-04 _ __:...:...__:;_;;.c...__c_ __
Level (low/med): Date Received: --~1~2~/~1~8~/~9~8'--
.• Solids:
'·•
0.0
Concentration Units (ug/L or mg/kg dry weight) : ____ u~g~/_L __ _
' ' !CAS No. Analyte
' ' ' :7429-90-5 Aluminum
'7440-36-0 Antimony
7440-38-2 Arsenic
7440-39-3 Barium
, 7440-41-7 Beryllium
17440-43-9 Cadmium
7440-70-2 Calcium
7440-47-3 Chromium
7440-48-4 'Cobalt
7440-50-8 Copper
7439-89-6 Iron
7439-92-1 Lead
7439-95-4 Magnesium
,7439-96-5 Manganese
17439-97-6 !Mercury
!7440-02-0 :Nickel
!7440-09-7 \Potassium 17782-49-2 !Selenium
7440-22-4 JSilver
7440-23-5 !Sodium
7440-28-0 !Thallium
7440-62-2 !Vanadium
7440-66-6 !Zinc
:cyanide f-------,
Color Before: 1 lor After:
' Comments:
----
' ' Concentration ' C Q '
' ' :
' ' ' ' '
'
4380
' ' ' 33.1 ' ' :
:
' '
'
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
SDG No.: 98P04(icp)
M
p
p
7 ' '
'
U.S. EPA -CLP
l
INORGANIC ANALYSIS DATA SHEET
00056
EPA SAMPLE NO.
t Name: I W-26 i
~E~C~KE=N~F~E~L~D~E~R.:....;I~N~C~·:_ __________ Contract:-=E=lc..::P~a~s~o_::E~n~e~r~g~y"--'------------'
L"ab Code: Case No.: _______ _ SAS No.: _______ _
l:trix (soil/water ) : water
Level (low/med):
'
lsolids:
'
a.a
Lab Sample ID: _ _::9=8=1=2=1=6=3_-~0~5-
Date Received: __ ~1~2~/~1~8~/~9~8:.,.._
Concentration Units (ug/L or mg/kg dry weight): ug/L ----"-=---
Concentration C Q
SDG No.: 98P04 (icp)
M
:7429-90-5 Aluminum
!7440-36-0 Antimony
!7440-38-2 Arsenic
!7440-39-3 Barium
0 7440-41-7 Beryllium 7 4 4 0-4 3-9 Cadmium '--------------------------'----'
I .,
7440-70-2 Calcium
7440-47-3 Chromium
7440-48-4 Cobalt
7440-50-8 Copper
, 7439-89-6 Iron
:7439-92-1 Lead
:7439-95-4 Magnesium
h439-96-5 Manganese
17439-97-6 Mercury
:7440-02-0 Nickel
h440-09-7 Potassium
h1s2-49-2 Selenium
j7440-22-4 Silver
!7440-23-5 Sodium
:7440-28-0 :Thallium
]7440-62-2 \vanadium
]7440-66-6 !Zinc
' !Cyanide '
' '
Color Before: ___ _
'lor After:
Comments:
I
23.4 B p
17. 4 p
' ; T ' ' !
' ! ' ; '
' ! ' ' '
' ' ' . ' ' !
' ' '
' ' ;
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
I
I 00057
U.S. EPA -CLP
1 EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Ip Name:
Lab Code:
ECKENFELDER INC. Contract: El Paso Energy =====;..;__;:_;_.:...;._ _________ _
Case No.: _______ _ SAS No.: ________ _
,,trix I soil/water l : .cw.=a.::t..ce.::.r __ _ Lab Sample ID: 9812163-06 --'----=-'-'----
L~vel (low/med): Date Received: 12/18/98 -----'----
,,Solids: 0.0
Concentration Units (ug/L or mg/kg dry weight): ug/L ---==---
, ,
:cAS : No. Analyte Concentration C Q
:
7429-90-5 Aluminum
7440-36-0 Antimony
7440-38-2 Arsenic
7440-39-3 Barium
7440-41-7 Beryllium
7440-43-9 Cadmium
!7440-70-2 Calcium
:7440-47-3 Chromium
!7440-48-4 Cobalt
17440-50-8 Copper
:7439-89-6 Iron 14300 ,
:7439-92-1 Lead
17439-95-4 Magnesium
17439-96-5 Manganese , 285
17439-97-6 Mercury
\7440-02-0 Nickel
17440-09-7 Potassium
:7782-4 9-2 Selenium ,
17440-22-4 Silver
:7440-23-5 , Sodium :
:7440-28-0 Thallium
!7440-62-2 Vanadium
]7440-66-6 Zinc , Cyanide
: ;
·I '
Color Before: Clarity Before: Texture: ----lolor After: Clarity After: Artifacts:
Comments:
FORM I -IN
W-18 s
SDG No.: 98P04 (icp)
M
p
p
!
' !
7 '
!
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
I
ECKENFELDER INC. Contract: El Paso Energy : ===="--"='---------
00058
EPA SAMPLE NO.
W-19s t Name:
Lab Code: Case No.: _______ _ SAS No.: _______ _ SDG No.: 98P04 (icp)
ltrix (soil/water): water
-~ Level (low/med):
Lab Sample ID: 9812163-07 -~-'-"==-'----
Date Received: __ ~1~2~/~1~8~/~9~8::__
l'solids: 0.0
' I
Concentration Units (ug/L or mg/kg dry weight) =---~u~g~/~L::_ __
I .,,
' '
It
CAS No. Analyte
7429-90-5 Aluminum
7440-36-0 Antimony
7440-38-2 Arsenic
7440-39-3 Barium
7440-41-7 Beryllium
,7440-43-9 Cadmium
\7440-70-2 Calcium
' '7440-47-3 Chromium
7440-48-4 Cobalt
7440-50-8 Copper
7439-89-6 Iron
7439-92-1 Lead
7439-95-4 Magnesium
7439-96-5 Manganese
7439-97-6 Mercury
: 7 4 4 0-02-0 Nickel
h440-09-7 Potassium
7782-49-2 Selenium
7440-22-4 Silver
7440-23-5 Sodium
7440-28-0 Thallium
7440-62-2 Vanadium
7440-66-6 Zinc
•Cyanide
' '
Color Before: ----
,, lor After:
Comments:
I
' ' ' ' ' ' Concentration ' C ' Q ' M ' ' ' ' '
' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' '
' 3260 p
74.4 ' p
I I
' ' ' ' ' I I
' ' ' :
; ' ' -,
' '
' !
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
00059 _,
I
U.S. EPA -CLP
l EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
lb Name: I W-9 s
~E~C~K=E~N~F~E=L=D~E=R.:....:I~N~C::.:.,. __________ contract:__::E~l'--"P~a~s~o'--"E~n~e~r~g~y'--'------------~
L'ab Code: Case No.: _______ _ SAS No.: _______ _
-ttrix (soil/water ) : water
Level (low/med): I Solids: _o;:_. o;:_ __ _
Lab Sample ID: _ __:9~8;1~2~1~6~3--0~8=--
Date Received: __ ~1~2~/~1~8~/~9~8;:__
II Concentration Units (ug/L or mg/kg dry weight) : ug/L
l1 CAS No. Analyte Concentration C Q
7429-90-5 Aluminum
I 7440-36-0 Antimony
7440-38-2 Arsenic
7440-39-3 Barium
7440-41-7 Beryllium ,,. 7440-43-9 Cadmium
7440-70-2 Calcium
7440-47-3 Chromium
7440-48-4 Cobalt
I 7440-50-8 Copper
7439-89-6 Iron 35600
7439-92-1 Lead .,, 7439-95-4 Magnesium
7439-96-5 Manganese 535 '
7439-97-6 Mercury 0.10 u
7440-02-0 Nickel
! I 7440-09-7 Potassium
7782-49-2 Selenium
7440-22-4 Silver !
7440-23-5 Sodium I ,, 7440-28-0 Thallium
7440-62-2 Vanadium
7440-66-6 Zinc
Cyanide
I
Color Before: Clarity Before: Texture:
-olor After: Clarity After: Artifacts: ,.
Comments:
I
I
l'l FORM I -IN
I !
' ' '
SDG No.: 98P04(icp)
98P07 (Hg).
"\
b,tr---'--19 ,,,J'l
I /"
Ml
p
' p
CV
I '
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
00060
EPA SAMPLE NO.
[
Name:
b Code:
I W-20 D
ECKENFELDER INC. Contract: El Paso Energy =====:.:....;:.;.;.;:..;...__________ -----'----'-'-'---'-· ------------'
Case No.: _______ _ SAS No.: _______ _
ltrix (soil/water ) : .;;w..::a..::t..::e::.r __ _
Level (low/med):
Lab Sample ID: _.....:.9.:.8..::1..::2::.1.:.63::.-_0:..9:__
Date Received: 12/18/98 ---'---'----
.Solids: 0.0
I
I
Concentration Units (ug/L or mg/kg dry weight): ___ ~u~g~/~L::._ __
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
, 7440-43-9
!7440-70-2
!7440-47-3
!7440-48-4
17440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
!7440-02-0
7440-09-7
7'.'82-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before:
' ' !Analyte
' ' ' :Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
:Copper
Iron
Lead
Magnesium
,Manganese
!Mercury
:Nickel ' : Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Cyanide
----"tlor After:
Comments:
I
I
pl
I
' ' Concentration C Q ' ' ' ' ' ' :
' ' ' ' ' ' '
12.0 B
0.24 ; B
;
'
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
SDG No.: 98P04(icp)
M
' ' ' :
' ' ' '
p
' ' ' p ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' .
I I ' '
I
I
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
ECKENFELDER INC. Contract: El Paso Energy ====-'-'--CC...'-----------
00061
EPA SAMPLE NO.
W-16 s lb Name:
Lab Code: Case No.: SAS No. : _______ _ SDG No.: 98P07 (Hg) --------ltrix (soil/water): ~w~a~t~e~r'---
Level (low/med):
Lab Sample ID: _ _:9~8~1~2~1~6~3_-~1~0-
Date Received: 12/18/98 --==.:..:....:...:. __
.Solids:
I
I
I
I
I
I
g
I
0.0
)
Concentration Units (ug/L or mg/kg dry weight) =---~u~g~/~L:..___ .-/Jf;'~-1/f
r -----,----~--------.----.--------,--, n,J7 , "
CAS No. Analyte
7429-90-5 Aluminum
7440-36-0 Antimony
7440-38-2 Arsenic
7440-39-3 Barium
7440-41-7 Beryllium
7440-43-9 Cadmium
7440-70-2 Calcium
7440-47-3 Chromium
7440-48-4 Cobalt
7440-50-8 Copper
7439-89-6 Iron
7439-92-1 Lead
7439-95-4 Magnesium
7439-96-5 Manganese
7439-97-6 Mercury
7440-02-0 Nickel
7440-09-7 Potassium
7782-49-2 Selenium
7440-22-4 Silver
7440-23-5 Sodium
7440-28-0 Thallium
7440-62-2 Vanadium
7440-66-6 ,Zinc
:cyanide
! '
'
'
Concentration C Q M
0.10 u cv:
' ' ' ' ' ' ' ' ' ; '
!
! !
Color Before: Clarity Before: Texture: ----tlor After: Clarity After: Artifacts:
Comments:
Di-----------
D
pl FORM I -IN
I
I
I
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
ECKENFELDER INC. Contract: El Paso Energy -=-===-==:.c....=.:...;_ _________ _
00062
EPA SAMPLE NO.
W-16 I t Name:
Lab Code: Case No.: ________ _ SAS No.: _______ _ SDG No.: 98P07 (Hg)
ltrix (soil/water
Level (low/med):
.Solids:
) : water
o.o
Lab Sample ID: _ _;;;_9~8~12~1~6~3~-~l~l=----
Date Received: 12/18/98 --~~"-'--:...;;.. __
I Concentration Units (ug/L or mg/kg dry weight): ____ u~g_/_L ___ _
I
I
I
I
I
I
I
' ' CAS No. ' !Analyte
:
7429-90-5 Aluminum
7440-36-0 Antimony
7440-38-2 Arsenic
7440-39-3 Barium
7440-41-7 Beryllium
7440-43-9 JCadmium
7440-70-2 Calcium
7440-47-3 Chromium
7440-48-4 Cobalt
7440"50-8 Copper
7439-89-6 Iron
7439-92-1 ILead ' 7439-95-4 [Magnesium
7439-96-5 :Manganese
7439-97-6 Mercury
7440-02-0 Nickel
7440-09-7 Potassium
7782-4 9-2 Selenium
7440-22-4 Silver
7440-23-5 Sodium
7440-28-0 :Thallium
7440-62-2 [Vanadium
7440-66-6 !Zinc
:cyanide >------<
Color Before: tlor After:
Comments:
' ' ' ' ' ' ' Concentration C ' ' ' ' Q ' ' ' ' ' ' ' ' : ' ' ' ' ' ' : ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' : '
' ' ' :
0 10 u
' ' ' ' ' ' ' ' ' ' i ' i :
: ' '
Clarity Before: Texture:
Clarity After: Artifacts:
M
' CV
'
1---------
pl FORM I -IN
B
I
I
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
00063
EPA SAMPLE NO.
lb Name:
l!b Code:
I W-28 i
..:E..:C~KE=N..:F..:E..:L..:D..:E~R'--'I~N~C~-'------------Contract:-=E.=l__::P..:a..:s..:oc_::E~n~e~r~g~yc...1. ___________ _,
Case No.: _______ _ SAS No.: _______ _
ltrix (soil/water
Level (low/med): I Solids:
) : water
0.0
Lab Sample ID: _ _:9..:8.=l.:;2.=1..:.7..:6_-.:.0.:.l_
Date Received: __ ..:l..:2..:./..:2~1..:./..:9..:8'---
I Concentration Units (ug/L or mg/kg dry weight) : ___ _:u~g~/..:L:.._ __
0
0
I
I
I
I
I
I
No.
:7429-90-5
17440-36-0
17440-38-2
:7440-39-3
\7440-41-7
!7440-43-9
:7440-70-2
:7440-47-3
'7440-48-4
7440-50-8
7439-89-6
7439-92-1
, 74 39-95-4
:7439-96-5
:7439-97-6
!7440-02-0
1J440-09-1
:7782-49-2
!7440-22-4 h44 □-23-s h44 □-za-o 17 62 2 440--
7440-66-6
Color Before:
:
\Analyte
!
Aluminum
Antimony
Arsenic
:Barium
lserylliurn
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
!Magnesium ' [Manganese
!Mercury
\Nickel
!Potassium
]Selenium
!Silver
!Sodium
]Thallium
:Vanadium
!Zinc
:cyanide
'
----tlor After:
Comments:
I
I
pl
I
Concentration
433
7 .1
I
i '
i !
: ' !
' : '
Clarity Before:
Clarity After:
FORM I -IN
C
8
' '
'
'
'
'
Q
Texture:
Artifacts:
SDG No.: 98P04 (icp)
M
p
p
' i
I
I 00064
I
U.S. EPA -CLP
1 EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
t Name: I W-AD
~E~C~KE=N~F~E~L~D~E~R..:....;I~N~C~·-_________ Contract:__:E~l:.....:P~a~s~o:.....:E~n~e~r~g~yL.l ___________ _,
Lab Code: Case No.: _______ _ SAS No.: _______ _
ltrix (soil/water): water
Level (low/med): I solids: 0.0
Lab Sample ID: 9812176-02 _...c...;._....::....C.---'---
Date Received: __ ~1~2~/~2~1~/~9~8:___
I Concentration Units (ug/L or mg/kg dry weight): ug/L ---==---
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
:7440-20-0
h440-62-2
h440-66-6 l '
' Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
,Iron
!Lead ' 'Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
I
I
jsilver
!Sodium
!Thallium
!Vanadium
1 Zinc
:cyanide C------'
Color Before: ----J1or After:
Comments:
I
Concentration C Q
' ' ' ' l ' ' ' ' l ' ' ' l ' ' ' ' ' ' ' ' l ' l
' ' ' ' ' ' ' ' ' l ' ' 8.2 ' B ' ' ' ' ' ' ' ' ' ' 0.13 ' B ' ' ' 0.10 ' u ' ' ' ' ' l
i
' ' ' ' ' '
' ' ' ' T
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
SDG No.: 98P04 (icp)
98P07(Hg)
M
' ' ' ' ' l
' ' ' ' ' ' ' ' l
' ' ' ' p
P,
CV
'
'
'
'
I
I
U.S. EPA -CLP
l
00065
EPA SAMPLE NO. I INORGANIC ANALYSIS DATA SHEET
I Name: I W-17 s
_E_C_KE=N_F_E_L_D_E_R_I_N_C_. ___________ Contract:-=E~l:.....:P~a~s~o:.....:E~n~e~r~g~y!.....l. ___________ _;
Lab Code: Case No.:
frix (soil/water): _w~•~t~e~r __ _
Level {low/med):
folids: 0.0
--------SAS No. : _______ _
Lab Sample ID:_:.....:9~8~1~2~1~7~6~-~0~3:....__
Date Received: __ ~1~2~/~2~1~/~9~8:..__
I Concentration Units (ug/L or mg/kg dry weight) =---~u~g~/~L:...._ __
I
I
I
I
I
I
I
I
' ' :CAS No.
7429-90-5
7440-36-0
:7440-38-2
:7440-39-3
!7440-41-7
!7440-43-9
7440-70-2
7440-47-3
7440-48-4
,7440-50-8
:7439-89-6
:7439-92-1
:7439-95-4 ' 17439-96-5
:7439-97-6
!7440-02-0 ' 17440-09-7 ' :7782-4 9-2
\7440-22-4
!7440-23-5
:7440-28-0
:7440-62-2
i7440-66-6
I !
Color Before:
Analyte
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Cyanide
----llor After:
Comments:
I
I
pl
I
Concentration
5100
699
0. 4 6
'
Clarity Before:
Clarity After:
FORM I -IN
C
' ' T '
' ! ' ' '
'
Q
Texture:
Artifacts:
' ' !
;
SDG No.: 98P04 (icp)
98P07 (Hg)
M
p
p
CV
! !
' I ' ;
' !
I
I 00066
I
U.S. EPA -CLP
1 EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
lab Name: ECKENFELDER INC. Contract: El Paso Energy ------------------
Lab Code: Case No.: _______ _ SAS No.: _______ _
Lab Sample ID: 981217 6-04 _ _;;_;;..;c.c..c._;;_--'---latrix (soil/water): _w~a_t~e~r;_ __
Level (low/med): D ate Received: 12/21/98 --~'----'-'----I Solids: 0.0
I
I
Concentration Units (ug/L_or mg/kg dry weight) : ___ ~u~g~/~L;_ __
I
I
I
I
I
I
I
CAS No. Analyte
7429-90-5 Aluminum
7440-36-0 Antimony
7440-38-2 Arsenic
7440-39-3 Barium
7440-41-7 Beryllium
7440-43-9 Cadmium
7440-70-2 Calcium
7440-47-3 Chromium
7440-48-4 Cobalt
,7440-50-8 Copper ' !7439-89-6 Iron
7439-92-1 Lead
7439-95-4 Magnesium
7439-96-5 Manganese
7439-97-6 Mercury
7440-02-0 Nickel
17440-09-7 Potassium
17782-49-2 Selenium
!7440-22-4 Silver
' ,7440-23-5 Sodium
!7440-28-0 Thallium
7440-62-2 Vanadium
7440-66-6 Zinc
f-------,Cyanide
Color Before:
Joler After:
Comments:
I
' ' : Concentration C Q ' ' :
' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' 344 ' ' ' : ' ' ' ' ' '
' 12.2 ' B ' ' ' : ' ' ' ' ' ' ' ' ' ' : ' ' ' ' ' I ' ' I ' ' ' '
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
W-32 i
SDG No.: 98P04 (icp)
M
' ' :
' ' ' ' ' ' ' ' ' ' ' ' ' ' :
p ' ' ' ' ' ' p ' ' ' ' :
' '
'
'
I
I
U.S. EPA -CLP
1 I INORGANIC ANALYSIS DATA SHEET
lb Name:
!b Code:
ECKENFELDER INC. Contract: El Paso Energy .=..::c=..::..::.:=:..:.....:=-:._ ______ _
Case No.: _______ _ SAS No. : _______ _
ltrix (soil/water): _w_a_t_e_r __ _
Level {low/med): I Solids: o.o
Lab Sample ID: _ _:9~8=1~2~1~8~2_-~D~l __
Date Received: --~1~2~/~2~2~/~9~8c__
I Concentration Units (ug/L or mg/kg dry weight): ug/L
I ' ' CAS No. !Analyte Concentration C Q
' :
7429-90-5 :Aluminum
I 7440-36-0 !Antimony
7440-38-2 1Arsenic
7440-39-3 Barium
,7440-41-7 Beryllium
I [7440-43-9 Cadmium
:7440-70-2 Calcium
!7440-47-3 Chromium
!7440-48-4 Cobalt
I !7440-50-8 !copper
7439-89-6 ' 3030 1Iron
7439-92-1 !Lead
7439-95-4 !Magnesium ' ,7439-96-5 I :Manganese 78.4 ' 17439-97-6 !Mercury
!7440-02-0 :Nickel
I
' '
I
17440-09-7 lPotassium
I ' ' '7782-4 9-2 JSeleniurn
7440-22-4 !Silver
7440-23-5 !Sodium
7440-28-0 !Thallium
I 7440-62-2 !Vanadium ' ' 7440-66-6 !Zinc
:cyanide
I
Color Before: Clarity Before: Texture: ----fior After: Clarity After: Artifacts:
Comments:
I
I
pl FORM I -IN
I
00067
EPA SAMPLE NO.
W-30 i
SDG No.: 98P04(icp)
) pt/..·✓p1, MJ:J/ y r
M
p
p
' '
I I ' '
I
I
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
00068
EPA SAMPLE NO.
t Name: I ~-10 i
cE=C=KE=N~F~E=L=D=E=R:c....=I~N=C~·-_________ contract:~E~l~P~a=s~o~E=n~e=r~g~y~'-----------__.J
Lab Code: ~se No.: _______ _ SAS No.: ________ _
lltrix (soil/water): water
Level (low/med):
lsolids: o.o
Lab Sample ID: _ __.c9~8~1_2~1~8~2_-~0~2 __
Date Received: 12/22/98 -----'----
n Concentration Units (ug/L or mg/kg dry weight) : ____ u~g~/~Lc__ __ _
D
0
u
I
I
I
I
' ' CAS No. !Analyte
' :
7429-90-5 :Aluminum
7440-36-0 !Antimony
7440-38-2 !Arsenic
7440-39-3 ' :Barium
7440-41-7 1 Bery 11 i urn
7440-43-9 Cadmium
7440-70-2 Calcium
7440-47-3 Chromium
7440-48-4 Cobalt
7440-50-8 Copper
7439-89-6 Iron
7439-92-1 Lead
7439-95-4 Magnesium
7439-96-5 Manganese
7439-97-6 :Mercury
7440-02-0 INickel
7440-09-7 Potassium
7782-4 9-2 Selenium
7440-22-4 Silver
7440-23-5 Sodium
7440-28-0 ,Thallium
7440-62-2 :vanadium ' 7440-66-6 !Zinc
' \cyanide ' ; '
Color Before: ___ _
.lor After:
Comments:
I
Concentration C Q
' '
' :
' ' 111 :
' :
' ' ' ' 4. 4 ' B ' ' ' '
I I ' '
'
'
'
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
SDG No.: 98P05(icp)
' ' M '
p
p
11 ' '
' '
' '
' '
' '
00069
I
I
I
U.S. EPA -CLP
1 EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
t Name:
!
~E::C:::K::;E:::N.:.F:.:E:::L::D:::E::Rc:..._::.IN=C.:.· __________ contract : El Paso Energy !
Lab Code: Case No.: _______ _ SAS No.: _______ _
1Jrix (soil/water ) : water
Level {low/med):
Lab Sample ID: _ _;;9~8~1~2~1~8~2_-~0~3-
Date Received: __ ~1~2~/~2~2~/~9~8:..__
lolids:
I
I
I
I
I
I
0.0
Concentration Units (ug/L or mg/kg dry weight): ug/L ---==---
CAS No. Analyte Concentration C Q
7429-90-5 Aluminum
7440-36-0 Antimony
7440-38-2 Arsenic
7440-39-3 Barium
:7440-41-7 Beryllium
!7440-43-9 Cadmium
17440-70-2 Calcium
\7440-47-3 Chromium
' '7440-48-4 Cobalt
7440-50-8 Copper
7439-89-6 Iron 70.6 B
7439-92-1 Lead
7439-95-4 ,Magnesium
:7439-96-5 I Manganese
' !7439-97-6 Mercury ' :7440-02-0 Nickel
' 11.0 ' B ' ' ! ' ' ' ' ' ' ' ' ' 7440-09-7 Potassium ' : !
' ' ' ' ' ' :
I
0
7782-49-2 Selenium : ' :
7440-22-4 Silver : ' ' 7440-23-5 Sodium ' ' '
7440-28-0 Thallium ' ' '
7440-62-2 Vanadium
7440-66-6 Zinc
:cyanide
I
Color Before: ___ _ Clarity Before: Texture:
J1or After: Clarity After: Artifacts:
Comments:
I
FORM I -IN
W-5 i
SDG No.: 98P05(icp)
M
p
p
:
:
;
;
; .
I
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
00070
EPA SAMPLE NO. I
t Name: I W-29 i
~E=C=KE=N~F~E=L=D=E=R:_I=N~C::..;_. __________ Contract:-=E~lc....;:P~a~s~oc....;:E=n~e=r~g~y'--'------------...l
Lab Code: Case No.: _______ _ SAS No.: _______ _ ltrix (soil/water): _w_a_t_e_r __ _ ·\Lab Sample rn·,·· 9812182-04
Level (low/med): Date Received: 12/22/98
lsolids: 0.0
I Concentration Units (ug/L or mg/kg dry weight): ---~u~g~/~L:_ __
I
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before:
Analyte
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium.
Vanadium
Zinc
Cyanide
!
----
' lor After:
Comments:
I
Concentration C Q
5.7 u
25.6
' ' '
I I !
' !
'
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
' !
'
I '
SDG No.: 98P05(icp)
M
p
p
' '
I : ;
!
"\
. I 'v r, ,/~ _,..~//t/ '1.'' 1/ I l"l'tf , /
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I U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
I Name: ECKENFELDER INC. Contract: El Paso Energy
Lab Code: lrix (soil/water
Level (low/med):
lolids:
I
Case No.: _______ _ SAS No.: _______ _
) : water Lab Sample ID: 9812182-05 ---....C.'-'----'-'--
Date Received: ___ 1_2_/_2_2~/_9_8 __
0.0
00071
EPA SAMPLE NO.
W-AC
SDG No.: 98P05(icp)
Concentration Units (ug/L or mg/kg dry weight): ug/L ---=.:....:: __ _
I CAS No.
I 7429-90-5
7440-36-0
7440-38-2
7440-39-3
u 7440-41-7
7440-43-9
7440-70-2
:7440-47-3
I 17440-48-4
7440-50-8
7439-89-6
7439-92-1
I 7439-95-4
7439-96-5
7439-97-6
7440-02-0
I 17440-09-7 ' '7782-49-2
7440-22-4
7440-23-5
I 7440-28-0
,7440-62-2
!7440-66-6
l
I
Color Before: llor After:
lmments:
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I
Analyte
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Cyanide
Concentration. C Q M
7.5 B p
26 2 p ' ' ' ' ' ' ' ' ' ' !
' ! ' ' ' ' 7 ' ' ' '
' ! ' '
' ! ' ' !
' '
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
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U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
00072
EPA SAMPLE NO.
lb Name: I W-22 s
ECKENFELDER INC. Contract: El Paso Energy ====::..::.:.....;:..:....:.....;__________ --'----'----'-'---'-·-----------'
Lab Code: Case No.:
ltrix {soil/water): water
Level (low/med): I Solids: o.o
--------SAS No.: _______ _ SDG No.: 98P05(icp)
Lab Sample ID: _ _::9..:8~1~2~1~8~2_-~0~6-
Date Received: 12/22/98 --~C....::.::..C..'-'----
'\ I Concentration Units (ug/L or mg/kg dry weight): ___ ..:u:..:gc:l..:L:___ · J#l'-< f9
,----~---,------~--~~-----~ j·l:,
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CAS No. Analyte
7429-90-5 Aluminum
7 4 4 0-3 6-0 Antimony
7440-38-2 Arsenic
7440-39-3 Barium
7440-41-7 Beryllium
7440-43-9 Cadmium
7440-70-2 Calcium
7440-47-3 Chromium
7440-48-4 Cobalt
7440-50-8 Copper
7439-89-6 Iron
7439-92-1 Lead
7439-95-4 Magnesium
7439-96-5 Manganese
7439 97 6 M --ercury
7440-02-0 Nickel
7440-09-7 Potassium
7782-49-2 Selenium
7440-22-4 Silver
7440-23-5 Sodium
7440-28-0 Thallium
7440-62-2 Vanadium
7440-66-6 Zinc
Cyanide
'
Color Before: ----lolor After:
Comments:
I
' ;
:
Concentration C Q M
5340 p
645 p
' ' ' ' :
' '
' ' '
' ' ' ' ' ! ' ' ' ' ! ' ' ' ' ' ' ;
' ' ' ;
; ! : :
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
U.S. EPA -CLP
l
INORGANIC ANALYSIS DATA SHEET
00073
EPA SAMPLE NO.
I
I
I
t Name: I W-22 i I
..::E:.::C::.KE:.::::.N:.::F..::E:.::L:.:D:.:E:.:R.:....:I:.:N:.:C:..·:__;_'-_______ con tract: -=E.;:l_:_P.;:a.;;s.;:o-=E::.n:.:e:.:rc,gc,yc...L ___________ __J .
Lab Code: _____ Case No. : _______ _ SAS No.: _______ _
ltrix (soil/water ) : water
Level (low/med): I solids: 0.0
Lab Sample ID:_-=9..::8..::l.;:2..::l.;:8.;:2_-.;:07.:__
Date Received: __ .;:l:.:2:.:l..::2:.:2:.:/~9:..8:__
I Concentration Units {ug/L or mg/kg dry weight) : ___ .;:u~g~/.;:L:_ __
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I
' ' :cAS i No.
' 7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
:7440-43-9
!7440-70-2
!7440-47-3
!7440-48-4
:7440-50-8
17439-89-6
h 4 3 9-92-1
:7439-95-4
17439-96-5
!7439-97-6
!7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
:7440-66-6
' !
!
Analyte
Aluminum
Antimony
:Arsenic
!Barium
!Beryllium ' ' 1Cadmium
' 'Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
,Nickel
:Potassium
:selenium
Silver
Sodium
Thallium
Vanadium
Zinc
,cyanide
'
Color Before: ___ _ lolor After:
Comments:
'
Concentration C Q
1320
22.2
' :
' ' ' ' '
Clarity Before: Texture:
Clarity After: Artifacts:
SDG No.: 98P05(icp)
M
p
p
' '
! ' : '
'
'
'
'
•~--------
FORM I -IN
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U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
00074
EPA SAMPLE NO. I
t Name: I W-AE
ECKENFELDER INC. Contract: El Paso Energy =_;_:;....:..=c..::.;_:;_;___________ -'----'--"-'---'--------------'
Lab Code: _____ Case No. : _______ _ SAS No.: --------frix (soil/water): ~w~a~t~e~r;_ __
Level {low/med):
lalids: 0.0
Lab Sample ID: 9812182-08 _....::..c.c:c.c.c.c.c.....:..;;__
Date Received: 12/22/98 ---'--"'--C...:...--
SDG No.: 98P05(icp)
I Concentration Units (ug/L or mg/kg dry weight) : ___ ~u~g~/~L:.._ __
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' ' ' ' lcAs No. !Analyte
' ' ' : ' :7429-90-5 Aluminum
17440-36-0 Antimony
:7440-38-2 Arsenic
,Barium !7440-39-3
' :7440-41-7 :Beryllium
!7440-43-9 'cadmium
:7440-70-2
07440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
17439-96-5
h439-97-6
!7~40-02-0
!7440-09-1
h1s2-49-2
h440-22-4
h440-23-s
h440-2s-o
17440-62-2
!7440-66-6 :
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Cyanide
Color Before:
f1or After:
Comments:
.I
I
i
----
' ' ' Concentration ' ' ' ' '
5.7
0.11
' '
Clarity Before:
Clarity After:
FORM I -IN
' ' : C
u
B
' '
I I
' '
' ' Q M ' ' ' '
:
:
:
:
p
! p
11
' '
Texture:
Artifacts:
I
I 00075
I
U.S. EPA -CLP
1 EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
t Name: 0E=C=K~E=N~F=E=L=D=E=R"--'I=N~C::..;_· __________ Contract: El Paso Energy
Case No.: Lab Code: --------SAS No.: _______ _
ltrix (soil/water): ~w~a=t=e=r:..._ __
Level (low/med): I Solids: 0.0
Lab Sample ID: 9812182-09 --------
Date Received: __ ~1=2=/~2=2=/~9=8'--
I Concentration Units (ug/L or mg/kg dry weight) : ____ u~g~/_L __ _
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I
r ' 1CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Analyte
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
,Calcium
' :Chromium
' :Cobalt ' :copper
:Iron ' :Lead ' !Magnesium
!Manganese
!Mercury
!Nickel
!Potassium
'Selenium
Silver
Sodium
Thallium
:Vanadium
!Zinc
:cyanide
Color Before: ___ _ tlor After:
Corrunents:
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I
pl
I
Concentration
1810
74.9
Clarity Before:
Clarity After:
FORM I -IN
' '
1
C Q
;
;
Texture:
Artifacts:
W-1 s
SDG No.: 98P05(icp)
M
p
p
:
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U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
ECKENFELDER INC; Contract: El Paso Energy ------------------
00076
EPA SAMPLE NO.
W-20 s t Name:
Lab Code: Case No.: _______ _ SAS No.: _______ _ SDG No.: 98P05(icp)
frix (soil/water): _w~a~t~e~r:..._ __
Level (low/med):
Lab Sample ID: 9812182-10 _ _,_c._.....;:.:..:;_.....;:.:...__
Date Received: 12/22/98 ----C."-'--'---
folids:
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I
I
I
I
0.0
Concentration Units (ug/L or mg/kg dry weight): ~g/L ---==---,,1,-,:,v
~----~----~--------~---~-------~~ 11, . .?t. ,_,,[ [,·
: l, ·'I ./LI] 1/ (
ICAS N A 1 t C t. C Q M ff :, o. na y e oncentra 1.on : / :
' '
)7429-90-5 Aluminum : ' ' ' '
:7440-36-0 Antimony : ' ' ' '
\7440-38-2 Arsenic ' ' : ' ' /7440-39-3 Barium ' : : ' !7440-41-7 Beryllium ' ' : ' '
:7440-43-9 Cadmium ' ' ' ' ' '
!7440-70-2 Calcium ' ' ' ' ' '
!7440-47-3 Chromium ' : : ' !7440-48-4 Cobalt ' : : ' 17440-50-8 Copper : ' ' ' '
7439-89-6 Iron 844 ' ' p ' ' ' '
7439-92-1 Lead : ' ' ' '
7439-95-4 Magnesium : : ' '
7439-96-5 Manganese 11. 6 ' B ' p ' ' ' '
7439-97-6 Mercury ' ' : ' ' 7440-02-0 Nickel
7440-09-7 Potassium
7782-49-2 Selenium i
7440-22-4 Silver
7440-23-5 Sodium
!7440-28-0 Thallium ! ' !7440-62-2 Vanadium ' ,
' '
17440-66-6 Zinc '
' Cyanide
Color Before: Clarity Before: Texture: ----
' lor After: Clarity After: Artifacts:
Comments:
I
FORM I -IN
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DATA VALIDATION REPORT
FCX Statesville
(FCX299B)
Prepared By
Environmental Data Services, Ltd.
For
Eckenfelder, Inc.
March 1, 1999
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DAT A ASSESSMENT NARRATIVES
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DATA ASSESSMENT NARRATIVE FOR VOLATILES
SITE: FCX Statesville
LABORATORY: Eckenfelder, Inc.
SAMPLE DELIVERY GROUP: FCX299B
This sample delivery group consists of the following water samples:
W-20i W-30i W-24s W-20i
W-BA W-24s W-BB Tri Blank 1-27-99
W-30i
Holdin Blank 1-27-99
Samples described above were analyzed via USEPA Low Level CLP SOW OLCD1 .0 to determine the
concentration of volatiles in water.
USEPA Contract Laboratory Program National Functional Guidelines for Organic Data Review (February
1994) have been considered during the validation of this data and in determining its usability.
All data are valid and acceptable except those analytes which have been qualified as described in the
attached glossary. All data qualification related to this group of samples is detailed on the attached
sheets.
Major Data Quality Issues
None.
Minor Data Quality Issues
Blank Contamination -Various target analytes were present in method, field and trip blanks associated
with samples in this delivery group. Effected compound results have been qualified per USEPA
guidelines.
Continuing Calibration -Two continuing calibrations had an observed percent difference for
bromomethane that failed to meet validation criteria. All sample analyses associated with the
non-compliant continuing calibrations have been flagged "UJ" estimated.
Two facts should be noted by all data users. First, the "R" flag means that the associated value is
unusable due to significant QC problems, the data is invalid and provides no information as to whether
the compound is present or not. "R" values should not appear on any data tables even as a last resort.
Lastly, strict QC serves to increase confidence in data but any value potentially contains error.
Date:
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HOLDING TIME
The amount of an analyte can change with time due to chemical instability, degradation, volatilization,
etc. If the specified holding time is exceeded the data may not be valid.
The analyses performed on samples in this sample delivery group were all done within established
holding times.
BLANK CONTAMINATION
Quality assurance blanks, method, trip, field, or rinse blanks are prepared to identify any contamination
which may have been introduced into the samples during preparation or field activity. Method blanks
measure lab contamination. Trip blanks measure cross contamination during shipment. Field and rinse
blanks measure cross contamination during field operations.
Method Blank Contamination
Method blanks were analyzed at the proper frequency. Upon examination, the method blanks did not
contain any target analyte at or above reportable concentration levels with the following exceptions.
The method blank performed on 1 /28/99 (VBLK0128A) was found to contain chloromethane (0.1 ug/I)
and methylene chloride (0.2 ug/I).
Larger amounts of methylene chloride were detected in the associated trip, holding and field blank
samples. Therefore the methylene chloride results associated with the method blank described above
were qualified based on those values. Sample W-30I (1-26-99) however was associated with the method
blank described above and had a chloromethane concentration in the effected range. Therefore,
chloromethane has been flagged "U" for sample W-30I (1-26-99).
The method blank performed on 1-29-99 (VBLK0129) was found to contain methylene chloride (0.08
ug/I). Larger amounts of methylene chloride were detected in the associated holding, trip and field
blanks. Therefore, methylene chloride results associated with method blank VBLK0129 were qualified
based on those results.
2
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Field Blank/Trip Blank/Holding Blank Contamination
Field, trip and holding blank sets were collected on 1-27-99.
Methylene chloride was found in the blanks collected on 1-27-99. The field blank contained methylene
c1loride at 0.3 ppb. The holding blank contained methylene chloride at 1 ppb. The trip blank contained
methylene chloride at 0.3 ppb. Per validation guidelines samples associated with the blanks .described
alJove were qualified based on the highest concentration blank. All samples in the delivery group were
a:;sociated with the blank samples collected on 1-27-99 and were found to contain comparable levels of
methylene chloride i.e. (less than 1 Ox the concentration of the blank). Methylene chloride results for the
samples listed have been flagged "U" not detected.
[]i-201 (1-26-99) I W-301 (1-26-99) I W-245 (1-26-99) I W-201 (1-27-99) I W-30I (1-27-99)
Tetrachloroethene (0.6 ppb} was positively identified in the field blank collected on 1-27-99.
The following samples were associated with the field blank sample described above and had
t, ,trachloroethene results in the effected concentration range.
[] /-245 (1-26-99) I W-245 (1-27-99) I W-BB
Tetrachloroethene results for the samples listed above were flagged "U" not detected.
!1IASS SPECTROMETER TUNING
Tuning and performance criteria are established to ensure adequate mass resolution, proper
i• lentification of compounds, and to some degree, sufficient instrument sensitivity. These criteria are not
1 ample specific. Instrument performance is determined using standard materials. Therefore, these
criteria should be met in all circumstances.
-,·he tuning standard for volatiles is bromofluorobenzene (BFB).
l•.1I tunes associated with this SDG were fully compliant.
CALIBRATION
!,atisfactory instrument calibration is established to ensure that the instrument is capable of producing
:1cceptable quantitative results. The initial calibration curve demonstrates that the instrument is capable
< ,f giving acceptable performance at the beginning of an analytical sequence. The continuing calibration
1•erifies that the instrument is giving satisfactory daily performance.
I::esponse Factor
· 'he response factor measures the instruments responses to specific chemical compounds. The response
I actors for the VOA Target Compound List must be greater than or equal to 0.05 in both the initial and
continuing calibrations. A value less than 0.05 indicates serious detection and quantitation problems.
l'!RF values in all initial and continuing calibrations were greater than 0.05.
3
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f'ercent Relative Standard Deviation (RSD) and Percent Deviation (¾D)
f'ercent RSD is calculated from the initial calibration and is used to indicate stability of a specific
compound over the calibration range. %D compares the respo'nse factor of the continuing calibration with
t 1e mean response factor of the initial calibration. Therefore %D is a measure of the instruments daily
1 •erformance.
The following QC criteria has been applied for this project:
~'., RSD of initial calibration must be <30.0 %
~:; D for continuing calibrations must be <25.0%
h value outside these limits indicates potential detection and quantitation errors. According to the
tlSEPA CLP National Functional Guidelines for Organic Data Review (2/94), all positive and non-detect
rnsults are flagged as estimated.
-,-he initial and continuing calibrations associated with this sample delivery group met all validation
criteria with the following exceptions.
;·he continuing calibration performed on 1/28/99 had an observed percent difference value for
t,romomethane (37.1 %) that fell outside validation acceptance criteria. The following sample analyses
,.iere associated with the calibration described above:
[J lolding Blank I Trip Blank I W-20I I W-301 I W-BA
Bromomethane results for the samples listed above have been flagged "UJ" estimated.
-,-he continuing calibration performed on 1-29-99 had an observed percent difference value for
t,romomethane (42.9%) that fell outside validation acceptance criteria. The following sample analyses
,.,ere associated with the calibration described above.
I W-24S (1-27-99) I W-88 j W-201 j W-301
1:~TERNAL STANDARDS PERFORMANCE
I 1ternal standard performance criteria is meant to ensure that the GC/MS sensitivity and response are
t :able during every experimental run.
The internal standard area count must not vary by more than a factor of two from the associated
continuing calibration standard. The retention time of the internal standard must not vary by more than
</-30 seconds from the associated continuing calibration standard. If the area count is outside the (-
i 0% -100%) range of the associated standard, all positive results for compounds quantitated using that
ttandard are qualified as estimated, and non detects as UJ, but only if area is< 50%.
I 1ternal standard recoveries observed in all samples and method blanks were within acceptable limits.
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~:URROGATES
/di samples and blanks are spiked with surrogate compounds prior to sample preparation and analyses to
£,valuate overall laboratory performance and efficiency of the analytical technique.
1\II samples and method blanks evaluated in this report had observed surrogate recoveries within the
nstablished limits.
, :OMPOUND IDENTIFICATION
·,tolatile
rcL compounds are identified on the GC/MS by using the analyte's relative retention time (RRT) and ion
;pectra. For the results to be a positive hit, the sample peak must be within:': 0.06 RRT units of the
,;tandard compound, and have an ion spectra which has a ratio of the primary and secondary ion
intensities within 20% of that in the standard compound. No analytes were qualified for compound
identification.
MATRIX SPIKE/MATRIX SPIKE DUPLICATE
The matrix spike and matrix spike duplicate are generated to determine the precision and accuracy of
the analytical procedure in a given matrix. This information may be used to qualify data.
No sample from this delivery group was analyzed as matrix spike/matrix spike duplicate pair. Therefore,
no evaluation of matrix specific precision and accuracy indicators could be performed.
Laboratory control samples were processed at a frequency of one per twelve hour analysis period. LCS
recoveries were well within acceptance limits in every case.
OTHER QC DATA OUT OF SPECIFICATION
None.
FIELD DUPLICATE
Samples W-24S (1-27-99) and W-BB comprise the field duplicate pair associated with samples in this
delivery group. Field precision exhibited was extremely good. The largest percent difference observed
for positively identified target analytes between either pair was less than 1 %. Field precision was
demonstrated to be well within acceptable tolerances.
SYSTEM PERFORMANCE AND OVERALL ASSESSMENT
Non-compliant continuing calibration and control blank contamination data quality issues were found to
impact the results reported. All other QC criteria appears to be acceptable.
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DATA ASSESSMENT NARRATIVE FOR METALS
SITE: FCX Statesville
LABORATORY: Eckenfe\der, Inc.
Validation Report: FCX299B
This sample delivery group consists of the following water samples:
II W-BA I W-24s I W-BB
The samples described above were analyzed for either total target analyte list metals or manganese and
iron as directed on the field COC. The analyses were performed based on methodologies outlined in the
USEPA CLP SOW 3/90.
"USEPA Contract Laboratory Program National Functional Guidelines for inorganic Data Review" (Feb.,
1994) were used to evaluate the data set.
All data are valid and acceptable except those analytes which have been qualified with a "J" (estimated),
or "R" (unusable). All action is detailed on the attached sheets.
Major Data Quality Issues
None.
Minor Data Quality Issues
ICP Serial Dilution -Two ana\ytes had an observed percent deviation value that fell outside validation
acceptance limits during the \CP serial dilution determination. Sample results associated with
the non-compliant serial dilution determination have been qualified as estimated.
Two facts should be noted by all data users. First, the "R" flag means that the associated value is
unusable. In other words, due to significant QC problems, the analysis is invalid and provides no
information as to whether the compound is present or not. "R" values should not appear on data tables
even as a last resort. The second fact to keep in mind is that no analyte concentration, even if it has
passed all QC tests, is guaranteed to be accurate. Strict QC serves to increase confidence in data but
any value potentially contains error.
Diane Waldschmidt ~,,,
Environrhenfal Scientist/Director
Date: ___ ,.-?...,.A'-'--v-'7..,..//,'------'-/.-'c?....._· _ 7'7
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HOLDING TIME
.•
The amount of an analyte in a sample can change with time due to chemical instability, degradation,
volatilization, etc. If the specified holding time is exceeded the data may not be valid. Those analytes in
the samples whose holding time has been exceeded will be qualified as estimated, or unusable when
grossly exceeded.
All analyses were completed well within acceptable holding times.
BLANK CONTAMINATION
Quality assurance blanks, method, trip, field, or rinse blanks are prepared to identify any contamination
which may have been introduced into the samples during sample preparation or field activity. Trip blanks
measure cross contamination during shipment. Field and rinse blanks measure cross contamination
during field operations.
Method Blank Contamination
Method blanks were evaluated at the proper frequency. The associated method blanks provided data
indicating no contamination was present.
Field or Rinse Blank Contamination
One equipment blank sample 0/V-BA) was collected in association with this delivery group. Upon
evaluation of the equipment blank data obtained, no analytes were found to be present at levels above
the CRDL.
CALIBRATION
Satisfactory instrument calibration is established to ensure that the instrument is capable of producing
acceptable quantitative data. The initial calibration curve and its verification demonstrates that the
instrument is capable of giving acceptable performance at the beginning of the analytical sequence. The
continuing calibration verification standards provide information as to the continuing stability of the
calibration curve.
Correlation Coefficient
All calibrations associated with the data represented here demonstrated satisfactorily that all criteria were
met.
Initial and Continuing Calibration Verification
All initial and continuing calibration verifications that bracketed sample analyses associated with the
sample delivery group were within acceptance limits.
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Initial and Continuing Calibration Blanks
All initial and continuing calibration blanks were evaluated and none associated with reported sample
results had observed analyte concentrations greater than the reported detection limits (positive or
negative).
MATRIX SPIKE/MATRIX SPIKE DUPLICATE
The matrix spike/matrix spike duplicate is generated to determine the long term precision and accuracy
of the analytical method in a given matrix. · ·
Sample W-24S was selected to be evaluated for water matrix effects. The precision and accuracy
indicators were within validation guidelines for both iron and manganese. Therefore, no qualification for
iron was necessary.
DUPLICATE
Precision between the MS/MSD pair was evaluated for sample W-24S. All precision indicators were
favorable during the evaluation of sample W-24S and its duplicate.
LABORATORY CONTROL SAMPLE
The Laboratory Control Sample is a quality control sample of known concentration which is processed
along with a batch of samples. The percent recovery of the LCS can be used to assess the accuracy of
the analytical procedure performed by a specific individual. during a specific time period, and utilizing the
same reagents and equipment as those used for sample analyses. The LCS data is independent of
sample matrix and the results may formulate a basis for qualification.
All associated laboratory control samples had observed percent recoveries well within the range
required.
ICP SERIAL DILUTION
Precision between diluted and non-diluted analyses was determined on sample W-24S.
The percent deviation values for iron (18.0%) and manganese (17.6%) fell above the allowable
validation criteria (10%). The following samples were associated and have results for iron and
manganese qualified as estimated (J).
W-BA W-BB W-24S
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CRDL
CRDL (2 times the CRDL) standards were analyzed as required during ICP analytical run sequences. Upon evaluation, the percent recoveries for iron and manganese CRDL standards were well within validation guidelines.
INTERFERENCE CHECK STANDARDS
Interference check standard analyses were performed at the proper frequency. Upon examination, the recoveries of iron and manganese were well within acceptable limits (80-120%) for both the initial and final ICSA/ICSAB determination.
FIELD DUPLICATE
Samples W-24s and W-88 comprise the field duplicate pair associated with this sample delivery group. The values between the two analyses were comparable. Relative percent difference values were less than 2% for both iron and manganese .
SYSTEM PERFORMANCE AND OVERALL ASSESSMENT
The laboratory attempted to perform the analyses evaluated according to USEPA CLP SOW 3/90. The following are procedural deficiencies not directly impacting data quality and therefore not previously discussed.
1. No unspiked sample duplicate was performed as required by CLP methodologies.
The analytical process was in control throughout the analysis of the samples in this delivery group. Data quality issues were related to sample matrix effects.
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GLOSSARY OF DATA QUALIFIERS
The material was analyzed for, but not detected, The associated numerical value is the sample
quantitation limit.
The associated numerical value is an estimated quantity.
The data are unusable (compound may or may not be present),
Presumptive evidence of the presence of the material,
Presumptive evidence of the presence of the material at an estimated concentration.
The material was analyzed for, but was not detected. The sample quantitation limit is an
estimated quantity,
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00019
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-20I
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
,Jab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0112101
'atrix: (soil/water)
ft,ample wt/vol:
WATER
25.00 (g/mL) ML
LOW
Lab Sample ID: 9901121-01
Lab File ID: 0112101
Date Sampled: 01/26/99
Date Analyzed: 01/28/99
Dilution Factor: 1.0
IJevel:
I \
5 Moisture: not dee.
(low/med)
j,c Column: DB-624 ID: 0.53 (mm)
~oil Extract Volume: (uL) ----Soil Aliquot Volume: ,,
,I~
'11
,1
,,!
..
:I
.,, ,,
I ,,,
I
I ·,,
CAS NO. COMPOUND
67-64-1---------Acetone
71-43-2---------Benzene
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulb.de
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlor~benzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
5.0
0.08
1.0
1.0
1.0
1.0
5.0
1. 0
0.4
1.0
1.0
1
1.0
1.0
1.0
1.0
0.1
0.1
0.09
0.3
1.0
0.6
156-59-2--------cis-l,2-Dichloroethene :2'1 ;¼
156-60-5--------trans-l,2-Dichloroethene 0.2
78-87-5---------1,2-Dichloropropane --16
10061-01-5------cis-l,3-Dichloropropene 1.0
10061-02-6------trans-l,3-Dichloropropene 1. 0
100-41-4--------Ethylbenzene --1.0
591-78-6--------2-Hexanone 5.0
75-09-2---------Methylene chloride .;;,o --0-.-\}.8.
108-10-1--------4-Methyl-2-pentanone 5.0
100-42-5--------Styrene 1. 0
79-34-5---------1,1,2,2-Tetrachloroethane 1.0 --
FORM I VOA
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00020
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-20I
•ILab
Lab
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No;: .·NA SDG No.: FCX.V0112101
.,Matrix: (soil/water)
-:: Sample wt/vol:
I.Level:
I .
·% Moisture: not dee.
(low/med)
~
WATER
25. 00 (g/mL) ML
LOW
,_GC Column: DB-624 ID: 0.53 (mm)
Soil Extract Volume, ____ (uL)
Lab Sample ID: 9901121-01
Lab File ID: 0112101
Date Sampled: 01/26/99
Date Analyzed: 01/28/99
Dilution Factor: 1.0
Soil Aliquot Volume: ,,
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
'
II
Ii ,,
iii
'M• ,.
·1
J ,,
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene ·
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
L/So 4W ·B-.D.
1.0 u
1.0 u
1. 0 u
3'-i . ,3-i I-& .0 '
1.0 u
1.0 u
I
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00048
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-30I
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
ii, . 11f:,ab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0112101
iif'1atrix: (soil/water)
l,ample wt/vol:
revel: (low/med)
, Moisture: not dee.
WATER
25. 00 (g/mL) ML
LOW
Lab Sample ID: 9901121-02
Lab File ID: 0112102
tc Column: DB-624 ID: 0.53 (mm)
Soil Extract Volume: (uL) ----
Date Sampled: 01/26/99
Date Analyzed: 01/28/99
Dilution.Factor: 1.0
Soil Aliquot Volume: ____ (uL)
·1·
I
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I
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
-------------------------,-------~---
67-64-1---------Acetone -----------71 -43 -

2

-

-

-

-

-

-

-

-

-
Benzene~----------
75-27-4---------Bromochloromethane
75-27-4---------Bromodichlorometha~n_e ___ _
75-25-2---------Bromoform 74-83-9---------Bromometh~a_n_e ________ _
78-93-3---------2-Butanone
75-15-0---------Carbon dis~u~l,f~i~a~e=-------
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene ----
75-00-3---------Chloroethane
67-66-3---------Chloroform ---------
74-87-3---------Chloromethane
124-48-1--------Dibromochloro_m_e7tTh~a-n_e ____ _
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene -----541-73-1--------1,3-Dichlorpbenzene
106-46-7--------1,4-Dichloro'benzene ____ _
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane ____ _
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-1,2-Dichloroetrh-e_n_e __ _
156-60-5--------trans-1,2-Dichloroethene
78-87-5---------l,2-Dichloropropane ___ -_-_-_-
10061-01-5------cis-1,3-Dichloropropene
10061-02-6------trans-1,3-Dichloroprope_n_e __
100-41-4--------Ethylbenzene _______ ===
591-78-6--------2-Hexanone
75-09-2---------Methylene ~cTh~r~o~r~i-a~e::---------
108-10-1--------4-Methyl-2-pentanone ___ _
100-42-5--------Styrene
79-34-5---------1,1,2,2--~T~e~t-r~a~c~h-lro~r~o~e--cetrh7a~n-e-:::_-:::_-=
FORM I VOA
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1.0 u
0.06 J
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0.4 J
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00049
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-30I
Name: ECKENFELDER INC. Contract: EL PASO ENERGY Lab
ILab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0112101
,~atrix: (soil/water)
lsample wt/vol:
.Level: (low/med)
--'%-Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
ID: O. 53 (mm) 'IGC Column: DB-624
Soil Extract Volume: (uL) ----
Lab Sample ID: 9901121-02
Lab File ID: 0112102
Date Sampled: 01/26/99
Date Analyzed: 01/28/99
Dilution Factor: 1.0
Soil Aliquot Volume: ----
I ,. CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I'
,I.)
t
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
I I t-"0
? ;;,_
-8-2-tr -5--l)
0.1 J
1. 0 u
0.2 J
,6-8--B-j)
0.2 J
1. 0 u
(uL)
I
00085
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-24S
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0112101
ftrix: (soil/wate~)
Sample wt/vol:
:Ivel: (low/med)
% Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
I Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9901121-03
Lab File ID: 0112103
Date Sampled: 01/26/99
Date Analyzed: 01/29/99
Dilution Factor: 1.0
?oil Extract Volume: (uL) Soil Aliquot Volume:
I ,,
\ --.....
t
' 11
'
I
I·
I
·1
I
'I
:1,
----
CAS NO. COMPOUND
67-64-1---------Acetone
71-43-2---------Benzene
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disuil:iae
56-23-5---------Carbon tetrachloriae
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorooenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans~l,2-Dichloroethene __
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1. 0
1.0
0.1
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.2
1.0
0.09
1.0
1.0
1.0
1.0
1.0
1. 0
5.0
75-09-2---------Methylene cnloriae d ,O ~ ,
108-10-1--------4-Methyl-2-pentanone
5.0
100-42-5--------Styrene
1.0
79-34-5---------1 1 2 2-Tetrachloroethane 1. 0
. I I I __
FORM I VOA
u u
u u u
u
u u u
u u
J u
u u u u
u u
J u
J u u
u u u
u
u -mu
u
u u
{,/./
I
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00086
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-24S
Name: ECKENFELDER INC. Contract: EL PASO ENERGY lab
.wab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0112101
11atrix: (soil/water)
'···Sample wt/vol: tevel: (low/med)
% Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
Lab Sample ID: 9901121-03
Lab File ID: 0112103
Date Sampled: 01/26/99
Date Analyzed: 01/29/99
Dilution Factor: 1.0 'tC Column: DB-624 ID: 0.53 (mm)
Soil Extract Volume: (uL) ----Soil Aliquot Volume: __ _cc_(uL)
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene /,0
108-88~3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
.g..,..a
0.05
1. 0
1.0
1.0
1.0
1.0
-if-
J u
u u u
u
Q ,,,(-fi
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t/
FORM 1 I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Jab Code: NA Batch No. : NA SAS No.: NA
00097
CLIENT SAMPLE NO.
W-20I
SDG No.: FCX.V0112101
Matrix: (soil/water) WATER
'lample wt/vol: 25. 00 (g/mL) ML
Level: (low/med) LOW I~ Moisture: not dee.
13C Column: DB-624 ID: 0.53 (mm)
Soil Extract Volume: (uL) -----
Lab Sample ID: 9901121-04
Lab File ID: 0112104D
Date Sampled: 01/27/99.
Date Analyzed: 01/29/99
Dilution Factor: 20.0
Soil Aliquot Volume:
I
I
I
I
I
' I
I
I
I
I
CAS NO. COMPOUND
67-64-1---------Acetone
71-43-2---------Benzene
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disull:iae
56-23-5---------Carbon tetrachloriae
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-D~bromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-l--------l,3-Dichlor9benzene
106-46-7--------1,4-Dichlordbenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans:l,2-Dichloroethene __
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloriae
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tecrachloroethane __
FORM I VOA
100 UD
20 UD
20 UD
20 UD
20 UD
20 UD
100 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
20 UD
24 D
20 UD
15 JD
20 UD
20 UD
20 UD
100 UD 40 .::;.. J&U
100 UD
20 UD
20 UD
00098
FORM 1 CLIENT SAMPLE NO.
I
I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-20I
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0112101
i/atrix: (soil/water)
.ample wt/vol:
lilf"'evel: . (low/med)
II Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
_,c Column: DB-624 ID: 0.53 (mm)
l,oil Extract Volume: (uL) ----
Lab Sample ID: 9901121-04
Lab File ID: 0112104D
Date Sampled: 01/27/99
Date Analyzed: 01/29/99
Dilution Factor: 20.0
Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene 380 D
108-88-3--------Toluene 20 UD
71-55-6---------1,1,l-Trichloroethane 20 UD
79-00-5---------1,1,2-Trichloroethane 20 UD
79-01-6---------Trichloroethene 29 D
75-01-4---------Vinyl chloride 20 UD
1330-20-7-------Xylene(total) 20 UD
FORM I VOA
I
I
I
W'ab
llab
FORM l
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA
00108
CLIENT SAMPLE NO.
W-30I
SDG No.: FCX.V0112101
[atrix: (soil/water)
Sample wt/vol:
WATER
25. 00 (g/mL) ML
LOW
Lab Sample ID: 9901121-05
Lab File ID: 0112105D
Date Sampled: 01/27/99
Date Analyzed: 01/29/99
Dilution Factor: 50.0
revel: (low/med)
~ Moisture: not dee.
IGC Column: DB-624 ID: 0.53 (mm)
Soil Extract Volume: ____ (uL) Soil Aliquot Volume: -----'-'-(uL)
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------carbon disulb.de
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
250 so so so so so
250 so so so so so so so so so so so so so so
50
42 so so so so
50
250
75-09-2---------Methylene chloride I CO :J.-'3-
108-10-1--------4-Methyl-2-pentanone 250
100-42-5--------Styrene so
79-34-5---------1,1,2,2-Tetrachioroethane __ 50
FORM I VOA
Q
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
JD
UD
UD
UD
UD
UD
UD
-cff)-()
UD
UD
UD
00109
FORM 1 CLIENT SAMPLE NO.
I
I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-30I
Lab
ILab
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0112101
Matrix: (soil/water)
lsample wt/vol:
•
Level: (low/med)
% Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
lsoil Extract Volume: (uL) ----
Lab Sample ID: 9901121-05
Lab File ID: 0112105D
Date Sampled: 01/27/99
Date Analyzed: 01/29/99
Dilution Factor: 50.0
Soil Aliquot Volume: --~(uL)
I.
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene 1100 D
108-88-3--------Toluene so UD
71-55-6---------1,1,1-Trichloroethane 50 UD
79-00-5---------1,1,2-Trichloroethane 50 UD
79-01-6---------Trichloroethene 85 D
75-01-4---------Vinyl chloride 50 UD
1330-20-7-------Xylene(total) 50 UD
FORM I VOA
I
I
I FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
00118
CLIENT SAMPLE NO.
W-BA
.ab
'lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0112101
ftatrix: (soil/water)
'\ample wt/vol:
level: (low/med)
~ Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
fc Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9901121-06
Lab File ID: 0112106
Date Sampled: 01/27/99
Date Analyzed: 01/28/99
Dilution Factor: 1.0
Soil Extract Volume: (uL) ----Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
67-64-1---------Acetone
71-43-2---------Benzene
CONCENTRATION UNITS:
(ug/L or _ug/Kg) UG/L
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoforrn
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disull':i.ae
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroforrn
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-D~bromo-3-chloropropane_
106-93-4--------1,2-D:i.bromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------l,4-Dichlor6benzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
5.0
1. 0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1. 0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1. 0
1.0
1. 0
1.0
1.0
1. 0
1.0
1.0
1.0
5.0
75-09-2---------Methylene chior:i.ae 0, J.. ;;J .c' 0 ~
108-10-1--------4-Methyl-2-pentanone 5.0
100-42-5--------Styrene 1.0
79-34-5---------1,1,2,2-Tetrachioroethane __ 1. 0
FORM I VOA
Q
u u
u u u u
u 1/J
u u
u u u u u
u u u
u u u
u u u
u u u
u u u
rJB-t1JJ u -
u
u
I
I
I
00119
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-BA
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0112101
.ratrix: (soil/water)
lample wt/vol:
ltevel: (low/med)
I Moisture: not dee.
WATER
25.00 (g/rnL) ML
LOW
~C Column: DB-624 ID: O. 53 (mm)
Lab Sample ID: 9901121-06
Lab File ID: 0112106
Date Sampled: 01/27/99
Date Analyzed: 01/28/99
Dilution Factor: 1.0
loil Extract Volume: (uL) ----Soil Aliquot Volume: --~-(uL)
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene C ·• , :, r-&-~
108-88-3------~-Toluene 1.0
71-55-6---------1,1,1-Trichloroethane 1.0
79-00-5---------1,1,2-Trichloroethane 1.0
79-01-6---------Trichloroethene 1.0
75-01-4---------Vinyl chloride 1.0
1330-20-7-------Xylene(total) 1.0
FORM I VOA
Q
J'B-&.;,
u u u u
u u
,.,5-1? l
1-/ r Oh·
'
I
I
00124
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-24S
Lab N~me: ECKENFELDER INC. Contract: EL PASO ENERGY
Jab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0112101
Matrix: (soil/water)
lample wt/vol:
lit'evel: (low/med)
&. Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
~C Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9901121-07
Lab File ID: 0112107
Date Sampled: 01/27/99
Date Analyzed: 01/29/99
Dilution Factor: 1.0
~oil Extract Volume: (uL) ----Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-D~bromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorooenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1. 0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.2
1.0
0.1
1.0
1.0
1.0
1.0
1.0
1.0
5.0
2.0
5.0
1;0
1.0
----
Q
u u u
u
u u u u
u u u u u
u u
u u u
u
J u
J u u u u
u
u u
u u u u
(uL)
00125
FORM 1 CLIENT SAMPLE NO.
I
I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-24S
if'ab
l,ab
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0112101
'
atrix: (soil/water)
ample wt:/vol:
l evel: (low/med)
Moisture: not dee.
WATER
25. 00 {g/mL) ML
LOW
a:,c Column: DB-624 ID: 0.53 (mm)
lloil Extract Volume: ____ (uL)
Lab Sample ID: 9901121-07
Lab File ID: 0112107
Date Sampled: 01/27/99
Date Analyzed: 01/29/99
Dilution Factor: 1.0
Soil Aliquot: Volume: __ ....:__ (UL)
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroet:hene i,o 0-:il -a-
108-88-3--------Toluene 1.0 u
71-55-6---------1,1,1-Trichloroet:hane 1.0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroet:hene 1.0 u
75-01-4---------Vinyl chloride 1.0 u
1330-20-7-------Xylene(t:ot:al) 1. 0 u
FORM I VOA
00134 I
I
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-BB
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
ILab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0112101
Matrix: (soil/water) WATER Lab Sample ID: 9901121-08
lsample wt/vol: 25.00 (g/mL) ML Lab File ID: 0112108
Level: (low/med) LOW
1% Moisture: not dee.
I GC Column: DB-624 ID: 0. 53 (mm)
Soil Extract Volume: (uL) ----
I CAS NO. COMPOUND
Date Sampled: 01/27/99
Date Analyzed: 01/29/99
Dilution Factor: 1.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
____ (uL)
~ ,; 5--1 .
"' 3 or Cf
Q
I
I
I
I
I
I
I
I
I
I
I
I
67-64-1---------Acetone
.71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulb.de
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-D~bromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
5.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u i/J
5.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
0.06 J
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
0.2 J
1.0 u
0.08 J
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
5.0 u
2.0 u
5.0 u
1.0 u
1.0 u
I
I
00135
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-BB
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0112101
_.ratrix: (soil/water)
&ample wt/vol:
level: (low/med)
~ Moisture: not dee.
WATER
25. 00 (g/rnL) ML
LOW
re Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9901121-08
Lab File ID: 0112108
Date Sampled: 01/27/99
Date Analyzed: 01/29/99
Dilution Factor: 1.0
Soil Extract Volume: (uL) -----Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene
108-88-3--------Toluene ------
71-55-6---------1,l,l-Trichloroethane
79-00-5---------1,1,2-Trichloroethane ___ _
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride-------
1330-20-7-------Xylene(total) --------
FORM I VOA
/.t,'...:J::
1.0 U
1.0U
1.0 U
1.0 U
1.0U
1. 0 U
Q
,:ii)\/
·1 ,I •
r; o r
{/
I
I
I
lab
ab
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA
00144
CLIENT SAMPLE NO.
TRIP BLA
NK #1227
SDG No.: FCX.V0112101
watrix: (soil/water)
'lamp le wt/vol:
WATER
25.00 (g/mL) ML
LOW
Lab Sample ID: 9901121-09
Lab File ID: 0112109
Date Sampled: 01/27/99
Date Analyzed: 01/28/99
Dilution Factor: 1.0
'eve~: (low/med)
~ Moisture: not dee.
lfC Column: DB-624 ID: 0.53 (mm)
~oil Extract Volume: ____ (uL) Soil Aliquot Volume:
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I
I
I
I
I
I
I
I
I
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorooenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene cliloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachioroethane __
FORM I VOA
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1. 0
1.0
1.0
1. 0
1.0
1. 0
1. 0
1.0
1.0
1.0
1.0
1. 0
1.0
5.0
0.3
5.0
1.0
1. 0
u
u u u u
u
u u u
u
u u u u
u u u
u u u
u u u u
u u u u
u
JB u
u u
00145
FORM 1 CLIENT SAMPLE NO.
I
I
I VOLATILE ORGANICS ANALYSIS DATA SHEET TRIP ELA
NK #1227
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.V0112101
iilatrix: (soil/water)
Lmple wt/vol:
11evel: (low/med)
I Moisture: not dee.
WATER
25.00 (g/mL) ML
LOW
if Column:· DB-624 ID: 0. 53 (mm)
,loil Extract Volume: ____ (uL)
Lab Sample ID: 9901121-09
Lab File ID: 0112109
Date Sampled: 01/27/99
Date Analyzed: 01/28/99
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene 1. 0 u
108-88-3--------Toluene 1.0 u
71-55-6---------1,1,1-Trichloroethane 1.0 u
79-00-5---------1,1,2-Trichloroethane 1. 0 u
79-01-6---------Trichloroethene 1.0 u
75-01-4---------Vinyl chloride 1. 0 u
1330-20-7-------Xylene(total) 1.0 u
FORM I VOA
I 00149
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I HOLDING B
LANK 01289
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
lab Code : NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0112101
Matrix: (soil/water)
lample wt/vol:
ti"evel: (low/med)
I Moisture: not dee.
WATER
25.00 (g/rnL) ML
LOW
111:'C Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9901121-10
Lab File ID: 0112110
.oil Extract Volume: (uL) ----
Date Sampled: 01/28/99
Date Analyzed: 01/28/99
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (UL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-1,2-Dichloroethene
156-60-5--------trans-1,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-1,3-Dichloropropene
10061-02-6---0 --trans-1,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
Q
5.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u I
5.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
5.0 u
1 JB
5.0 u
1. 0 u
1.0 u
00150
FORM 1 CLIENT SAMPLE NO.
I
I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
HOLDING B
LANK 01289
•
Lab
Lab
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V0112101
IMatrix: (soil/water)
Sample wt/vol:
'
Level: (low/med)
% Moisture: not dee.
WATER
25. 00 (g/mL) ML
LOW
I GC Column: DB-624 ID: 0. 53 (mm)
Soil Extract Volume: (uL) ----
Lab Sample ID: 9901121-10
Lab File ID: 0112110
Date Sampled: 01/28/99
Date Analyzed: 01/28/99
Dilution Factor: 1.0
Soil Aliquot Volume:
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene 1. 0 u
108-88-3--------Toluene 1. 0 u
71-55-6---------1,1,1-Trichloroethane 1.0 u
79-00-5---------1,1,2cTrichloroethane 1.0 u
79-01-6---------Trichloroethene 1.0 u
75-01-4---------Vinyl chloride 1.0 u
1330-20-7-------Xylene(total) 1.0 u
FORM I VOA
U.S. EPA -CLP
1 I
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INORGANIC ANALYSIS DATA SHEET
Lab Name: ECKENFELDER INC. Contract: El Paso Energy
I Lab Code: ______ Case No. : ________ _ SAS No.: _______ _
Matrix (soil/water ) : water _;....:....~---I Level (low/med):
Lab Sample ID: _.....::.9~9~0~1~1~2~1_-~0~6 __
Date Received: 01/28/99 __ ....:........:...._c.,_.;_ __
I % Solids: 0.0
00006
EPA SAMPLE NO.
W-BA
SDG No.: 99P01
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Concentration Units (ug/L or mg/kg dry .weight): ug/L ---~"'-----
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Color
Color
' ' \CAS No.
' ' '
' ' lAnalyte
' ' ' 17429-90-5 \Aluminum
!7440-36-0 !Antimony
\7 4 4 0-38-2 \Arsenic
!7440-39-3 JBarium
!7440-41-7 !Beryllium
\7440-43-9 \Cadmium
!7440-70-2 !calcium
!7440-47-3 \Chromium
!7440-48-4 !cobalt
!7440-50-8 !copper
17439-89-6 lrron
\7439-92-1 !Lead
!7439-95-4 !Magnesium
!7439-96-5 \Manganese
17439-97-6 !Mercury
!7440-02-0 !Nickel
!7440-09-7 \Potassium
17782-49-2 !selenium
:7440-22-4 !Silver
!7440-23-5 \Sodium
\7440-28-0 !Thallium
!7440-62-2 lvanadium
:7440-66-6 !zinc
1....:....----~lcyanide
Before:
After:
Comments:
Concentration C Q M
9.3 u E p .1
0.38 B E p 1
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
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Lab Name:
U.S. E?A -CLP
1
INORGANIC ANALYSIS DATA SHEET
ECKENFELDER INC. Contract: El Paso Energy -=-=='-'-'=="--.C....:------------
00007
EPA SAMPLE NO.
W-24s
I Lab Code: Case No.: --------SAS No.:--------SDG No.: 99P01
I Matrix (soil/water ) :
Level (low/med): _____ _
water Lab Sample ID:
Date Received:
I % Solids: 0.0
I Concentration Units (ug/L or mg/kg dry weight) :
I ' ;
' ' !cAS No. \Analyte
' ' '
I 7429-90-5 jAluminurn
7440-36-0 JAntimony
:7440-38-2 !Arsenic
:7440-39-3 !Barium
I !7440-41-7 !Beryllium
:7440-43-9 !cadmium
\7440-70-2 !calcium
I
!7440-47-3 \Chromium
!7440-48-4 !cobalt
[7440-50-8 !copper
:7439-89-6 \Iron
:7439-92-1 ' I :Lead
!7439-95-4 \Magnesium
[7439-96-5 !Manganese
:7439-97-6 !Mercury
I [7440-02-0 lNickel
:7440-09-7 !Potassium
:7782-49-2 !selenium
I :7440-22-4 ! Silver
[7440-23-5 ]Sodium
:7440-28-0 !Thallium
[7440-62-2 !vana.dium
I :7440-66-6 !zinc
' !cyanide ' '
I Color Before: ----1 Color After:
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Comments:
Concentration C
55800
1780
Clarity Before:
Clarity After:
FORM I -IN
9901121-07 ---------
01/28/99 ---------
ug/L 1' .. I
~J)lV ·9'! I ., /, ,,, .... ,,,....,
I'
Q M
E p ,j
E p -r ,·
Texture:
Artifacts:
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Lab Name:
I Lab Code:
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
ECKENFELDER INC. Contract: El Paso Energy --------------------
00008
EPA SAMPLE t,;O.
W-BB
Case No.: --------SAS No.:_________ SDG No.: 99P01
I Matrix (soil/water ) : water
Level (low/med):
Lab Sample ID: 9901121-08
Date Received: 01/28/99
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% Solids: 0.0
,I '
Concentration Units (ug/L or mg/kg dry weight): ug/L -015/L·. ,,c,
~----~-----~--------~---~---_-_-_-_-_-_--:__'""_-_-_-_-_-_--:__-_-~-~ :"'; , f,. t.:.· ~· / f
' ' !cAS No. Analyte Concentration C Q M
' ' ' :7429-90-5 Aluminum
\7440-36-0 Antimony
\7440-38-2 Arsenic
!7440-39-3 Barium
\7440-41-7 Beryllium
l 7 4 4 0-4 3-9 Cadmium
\7440-70-2 Calcium
\7440-47-3 Chromium
!7440-48-4 Cobalt
\7440-50-8 Copper
\74 39-8 9-6 Iron 56900 E
\7439-92-1 Lead
:7439-95-4 Magnesium ' . \7439-96-5 Manganese
\7439-97-6 Mercury
p .r .---------i------,-----------i---..; 1770 E
\7440-02-0 Nickel
\7440-09-7 Potassium
!7782-49-2 Selenium
!7440-22-4 Silver
\7440-23-5 Sodium
\7440-28-0 Thallium
\7440-62-2 Vanadium
\7440-66-6 Zinc
' Cyanide ' '
Color Before: Clarity Before: Texture:
Color After: Claocity After: Artifacts:
Comments:
FORM I -IN
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DATA VALIDATION REPORT
FCX Statesville
(FCX299C)
Prepared By
Environmental Data Services, Ltd.
For
Eckenfelder, Inc.
March 1, 1999
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DATA ASSESSMENT NARRATIVES
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DATA ASSESSMENT NARRATIVE FOR VOLATILES
SITE: FCX Statesville
LABORATORY: Eckenfelder, Inc.
SAMPLE DELIVERY GROUP: FCX299C
This sample delivery group consists of the following water samples:
Wooten Well Hinson Well EC fi>W-31i W-32i
Trio Blank #1159 Trio Blank #1158 Holdina Blank 11/23198 Holdina Blank 11120198
W-31S Ouoe
W-31i
W-31S
Samples described above were analyzed via USEPA Low Level CLP SOW OLC01 .0 to detennine the
concentration of volatiles in water.
USEPA Contract Laboratory Program National Functional Guidelines for Organic Data Review (February
1994) have been considered during the validation of this data and in detennining its usability.
All data are valid and acceptable except those analytes which have been qualified as described in the
attached glossary. All data qualification related to this group of samples is detailed on the attached
sheets.
Major Data Quality Issues
Calibration -The initial calibration had an observed average relative response factor value for 1,2-
dibromo-3-chloropropane that failed to meet acceptable validation criteria. All associated
samples were non-detected for the effected compound. Therefore, the results have been
qualified unusable (R).
Minor Data Quality Issues
Blank Contamination -One common laboratory contaminant was present in equipment, holding and trip
blanks associated with samples in this delivery group. Effected compound results have been
qualified per USEPA guidelines.
Two facts should be noted by all data users. First, the "R" flag means that the associated value is
unusable due to significant QC problems, the data is invalid and provides no infonnation as to whether
the compound is present or not. "R" values should not appear on any data tables even as a last resort.
Lastly, strict QC serves to increase confidence in data but any value potentially contains error.
~;~
En if mental Scientist/Director
Date:
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HOLDING TIME
The amount of an analyte can change with lime due to chemical instability, degradation, volatilization, etc.
If the specified holding time is exceeded the data may not be valid.
The analyses perfonmed on samples in this sample delivery group were all done within established
holding times.
BLANK CONTAMINATION
Quality assurance blanks, method, trip, field, or rinse blanks are prepared to identify any contamination
which may have been introduced into the samples during preparation or field activity. Method blanks
measure lab contamination. Trip blanks measure cross contamination during shipment. Field and rinse
blank~ measure cross contamination duri_ng field operations.
Method Blank Contamination
Method blanks were analyzed at the proper frequency. Upon examination, the method blanks did not
contain any target analyte at or above reportable concentration levels.
Holding blanks 11/20/98 & 11/23/98 contained methylene chloride (0.22 ppb and 0.18 ppb respectively).
See blank section below for contamination details.
Field BlankfTrip Blank Contamination
Trip and equipment blank sets were collected on 11-19-98 and 11-20-98 which contained some target
analytes (see blank details below).
Qualification is based upon a comparison with the associated blank having the highest concentration of a
contaminant. If the sample concentration is less than 1 Ox for common contaminants i.e., methylene
chloride, and Sx for all other compounds, the compound result is flagged "U" not detected.
Blank Methylene Chloride Xylene
Trip Blank 1158 (11-20-98) 1.2 ppb ND
Trip Blank 1159(11-19-98) 0.96 ppb 0.30 ppb
Holding Blank (11-20-98) 0.22 ppb ND
Holding Blank (11-23-98) 0.18ppb ND
EB @W-311 0.46 ppb ND
All samples associated with non-compliant blanks were non-detected for methylene chloride and xylene
with the exception of W-31I for methylene chloride. Sample W-31 i had methylene chloride in the effected
concentration range. Therefore the methylene chloride result has been flagged "U".
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MASS SPECTROMETER TUNING
Tuning and perfonnance criteria are established to ensure adequate mass resolution, proper identification
of compounds, and to some degree, sufficient instrument sensitivity. These criteria are not sample
specific. Instrument perfonnance is detennined using standard materials. Therefore, these criteria should
be met in all circumstances.
The tuning standard for volatiles is bromofluorobenzene (BFB).
All of the tunes associated with this SDG were fully compliant.
CALIBRATION
Satisfactory instrument calibration is established to ensure that the instrument is capable of producing
acceptable quantitative results. The initial calibration curve demonstrates that the instrument is capable of
giving acceptable perfonnance at the beginning of an analytical sequence. The continuing calibration
verifies that the instrument is giving satisfactory daily perfonnance.
Response Factor
The response factor measures the instruments responses to specific chemical compounds. The response
factors for the VOA Target Compound List must be greater than or equal to 0.05 in both the initial and
continuing calibrations. A value less than 0.05 indicates serious detection and quantitation problems.
RRF values in all initial and continuing calibrations were greater than 0.05 with the following exceptions.
The initial calibration perfonned on 11 /24/98 had an observed average relative response factor value for
1-2-dibromo-3-chloropropane (0.049) that failed to meet validation acceptance criteria.
All associated samples were non-detected for 1,2-dibromo-3-chloropropane. Therefore, the resulls have
been qualified as unusable (R).
Percent Relative Standard Deviation (RSD) and Percent Deviation (%D)
Percent RSD is calculated from the initial calibration and is used to indicate stability of a specific
compound over the calibration range. %0 compares the response factor of the continuing calibration with
the mean response factor of the initial calibration. Therefore %0 is a measure of the instruments daily
perfonnance.
The following QC criteria has been applied for this project:
% RSD of initial calibration must be <30.0 %
% D for continuing calibrations must be <25.0%
A value outside these limits indicates potential detection and quantitation errors. According to USEPA
Contract Laboratory Program National Functional Guidelines for Organic Data Review, February, 1994 all
positive and not detected results are flagged as estimated.
The initial and continuing calibrations associated with this sample delivery group met all validation
criteria.
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INTERNAL STANDARDS PERFORMANCE
Internal standard perfonnance criteria is meant to ensure that the GC/MS sensitivity and response are
stable during every experimental run.
The internal standard area count must not vary by more than a factor of two from the associated
continuing calibration standard. The retention time of the internal standard must not vary by more than +/-
30 seconds from the associated continuing calibration standard. If the area count is outside the (-50% -
100%) range of the associated standard, all positive results for compounds quantitated using that
standard are qualified as estimated, and non detects as UJ, but only if area is< 50%.
Internal standard recoveries observed in all samples and method blanks were within acceptable limits.
SURROGATES
All samples and blanks are spiked with surrogate compounds prior to sample preparation and analyses to
evaluate overall laboratory perfonnance and efficiency of the analytical technique.
All samples and method blanks evaluated in this report had observed surrogate recoveries within the
established limits.
COMPOUND IDENTIFICATION
Volatile
TCL compounds are identified on the GC/MS by using the analyte's relative retention time (RRT) and ion
spectra. For the results to be a positive hit, the sample peak must be within :t 0.06 RRT units of the
standard compound, and have an ion spectra which has a ratio of the primary and secondary ion
intensities within 20% of that in the standard compound. No analytes were qualified for compound
identification.
MATRIX SPIKE/MATRIX SPIKE DUPLICATE
The matrix spike and matrix spike duplicate are generated to detennine the precision and accuracy of the
analytical procedure in a given matrix. This infonnation may be used to qualify data.
No sample was analyzed as the matrix specific (matrix spike analyses). Therefore, no matrix specific
analyses could be evaluated.
LABORATORY CONTROL SAMPLE
Laboratory control samples were processed at a frequency of one per twelve hour analysis period. LCS
recoveries were well within acceptance limits.
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OTHER QC DATA OUT OF SPECIFICATION
None.
FIELD DUPLICATE
Samples W-31s/W-31s Dupe comprise the field duplicate pair associated with samples in this delivery
group. Field precision exhibited was extremely good. The largest percent difference observed for
positively identified target analytes between either pair was 15%. Field precision was demonstrated to be
well within acceptable tolerances.
SYSTEM PERFORMANCE AND OVERALL ASSESSMENT
Control blank contamination data quality issues were found to impact the results reported. All other QC
criteria appears to be acceptable.
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DATA ASSESSMENT NARRATIVE FOR PESTICIDE
SITE: FCX Statesville
LABORATORY: Eckenfelder, Inc.
SAMPLE DELIVERY GROUP: FCX299C
This sample delivery group consists of the following water samples:
W-31s W-31s Du EB W31I
W-32I Wooten Well Hinson Well
W-31I
Samples described above were analyzed via CLP SOW OLC01.0 Protocol to determine the
concentrations of Pesticides and PCB's in water.
USEPA Contract Laboratory Program National Functional Guidelines for Organic Data Review (February
1994) have been considered during the validation of this data and in determining its usability.
All data are valid and acceptable except those analytes which have been qualified as described in the
attached glossary. All data qualification related to this group of samples is detailed on the attached
sheets.
Major Data Quality Issues
None.
Minor Data Quality Issues
Dual Column Analyses -The percent difference observed between sample results quantitated on
separate analytical columns was very large in several cases. The effected sample results were
qualified "J" or "JN" as appropriate.
Calibration -One compound had observed relative standard deviation values during the initial calibration
on both analytical columns that did not meet validation acceptance criteria. All sample analyses
were associated with the calibration and results for the effected compound have been flagged
estimated "J"rUJ".
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Two facts should be noted by all data users. First, the "R" flag means that the associated value is
unusable due to significant QC problems, the data is invalid and provides no information as to whether
the compound is present or not. "R" values should not appear on any data tables even as a last resort.
Lastly, no analyte concentration, even if it passed all QC tests, is guaranteed to be accurate. Strict QC
serves to increase confidence in data but any value potenflal\y contains error.
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HOLDING TIME
The amount of an analyte in a sample can change with time due to chemical instability, degradation,
volatilization, etc. If the specified holding time is exceeded, the data may not be valid. Those analytes
detected in the samples whose holding time has been exceeded will be qualified as estimated, "J". The
non-detects (sample quantitation limits) will be flagged as estimated, "J", or unusable, "R", if the holding
times are grossly exceeded.
All samples were prepared and analyzed within allowable holding time.
BLANK CONTAMINATION
Quality assurance (QA) blanks, i.e., method, trip, field, or rinse blanks are prepared to identify any
contamination which may have been introduced into the samples during sample preparation or field
activity. Method blanks measure laboratory contamination. Trip blanks measure cross-contamination of
samples during shipment. Field and rinse blanks measure cross-contamination of samples during field
operations. If the concentration of the analyte is less than 5 times the blank contaminant level (1 O times
for the common contaminants), the analytes are qualified as non-detects, "U".
Method Blank Contamination
A method blank was analyzed at the proper frequency. No target compounds were detected above the
associated reporting limits in the method blank.
Field or Rinse Blank Contamination ("water blanks" or "distilled water blanks" are validated like any
other sample)
A field blank was collected and analyzed in association with the samples in this delivery group. Upon
examination, no target compounds were detected above the reporting limit in the field blank.
CALIBRATION
Percent Relative Standard Deviation (¾RSD) and Percent Difference (¾D)
Percent RSD is calculated from the initial calibration and is used to indicate the stability of the specific
compound response factor over increasing concentration. Percent D compares the response factor of
the continuing calibration check to the mean response factor (RRF) from the initial calibration. Percent D
is a measure of the instrument's daily performance. For the PESTICIDE fraction, if% RSD exceeds
20% for all analy1es except for the 2 surrogates (which must not exceed 30% RSD) or %D exceeds 25%
for any analy1e, qualify all associated positive results "J" and non-detects "UJ". If %RSD and %D grossly
exceed QC criteria, non-detect data may be qualified "R".
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A four-point initial calibration curve was used per SOWOLC02.0 for the pesticides. Initial calibration
standards were complete for each column. Pesticides in each .level of the Individual Mixtures of A & B
fell within the retention time window established during the initial calibration.
The relative standard deviation values for all analytes on both analytical columns were within validation
guidelines with one exception: alpha-BHC had observed percent relative standard deviation values on
both analytical columns in excess of 20%. All samples in the delivery group are associated with the
calibration described above and sample results for the effected compound have been flagged as
estimated.
Continuing calibrations were analyzed at the proper frequencies and all observed percent difference
values met validation criteria for the compounds reported.
SURROGATES/SYSTEM MONITORING COMPOUNDS (SMC)
All samples are spiked with surrogate/SMC compounds prior to sample preparation to evaluate overall
laboratory performance and efficiency of the analytical technique. If the measured surrogate/SMC
concentrations were outside contract specifications, qualifications were applied to the samples and
analytes as shown below.
Surrogate recovery summaries were present for all samples. No sample results were qualified based on
observed surrogate recoveries because in no case were both surrogates outside limits.
COMPOUND IDENTIFICATION
Pesticide Fraction
The retention times of reported compounds must fall within the calculated retention time windows for the
two.chromatographic columns. The percent difference (%D) of the positive results obtained on the two
GC columns should be ,'.':25%.
Retention Time
All positively identified pesticide sample results reported fell within the daily retention time windows per
method guidelines.
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Percent Difference
Several sample analyses associated with this SDG had at least one positively identified compound that
required one of the following data qualifiers due to percent difference between results of the two
analytical columns that were extremely large.
= Estimated J
JN = Presumptive evidence of presence at an estimated concentration.
The following samples had unique identification difficulties and are described in detail below.
Sample Analyte qualifier
W-31s Dupe Delta-BHC J
W-32I Aldrin J
4,4'-DDD J
Endosulfan I J
Gamma-chlordane J
MATRIX SPIKE/SPIKE DUPLICATE, MS/MSD
The MS/MSD data are generated to determine the long-term precision and accuracy of the analytical
method in various matrices. The MS/MSD may be used in conjunction with other QC criteria for some
additional qualification of data.
No sample from this delivery group was analyzed as a MS/MSD pair. Therefore, matrix specific
precision and accuracy performance criteria could not be evaluated.
A laboratory control sample was processed along with the samples in this delivery group. All accuracy
indicators were favorable for the LCS determination.
No data qualifications have been applied based on the MS/MSD observations.
OTHER QC DATA OUT OF SPECIFICATION
None.
REPORTING
This package does not contain re-extraction, re-analysis or dilution. Form 1 'shave been documented to
clearly indicate the sample results to be reported.
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FIELD DUPLICATE
Samples W-31 Dupe and W-31s were collected as a field duplicate pair. Low level concentrations of
alpha-chlordane and delta-BHC were found in W-31s Dupe. No target analytes were positively reported
in W-31s. However, the values reported for each of the samples differed by less than the CRQL.
Therefore, overall the two data sets were found to be in good agreement.
SYSTEM PERFORMANCE AND OVERALL ASSESSMENT
The overall data for Pesticides/PCB's via SOW OLC02.0 met method acceptance criteria. -
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D
DATA QUALIFIER DEFINITIONS
The following definitions provide brief explanations of the national qualifiers assigned to results in the
data review process. If the Regions choose to use additional qualifiers, a complete explanation of those
qualifiers should accompany the data review.
U -The analyte was analyzed for, but was not detected above the reported sample
quantitation limit.
J -The analyte was positively identified; the associated numerical value is the
approximate concentration of the analyte in the sample.
N -The analysis indicates the presence of an anlayte for which there is presumptive
evidence to make a "tentative identification."
NJ The analysis indicates the presence of an analyte that has been "tentatively
identified" and the associated numerical value represents its approximate
concentrations.
UJ The analyte was not detected above the reported sample quantitation limit.
However, the reported quantitation limit is approximate and may or may not
represent the actual limit of quantitiation necessary to accurately and precisely
measure the analyte in the sample.
R -The sample results are rejected due to serious deficiencies in the ability to
analyze the sample and meet quality control criteria. The presence or absence
of the analyte cannot be verified.
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LABORATORY DAT A WITH QUALIFIERS ADDED
I FORM l CLIENT SAMPLQCW~S
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
W-32I
Lab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vlll5701
IMatrix: (soil/water) WATER Lab Sample ID: 9811174-0l
Sample wt/vol: 25.00 (g/mL) ML Lab File ID: 1117401
ILevel: (low/med) LOW Date Sampled: 11/20/98
1 % Moisture: not dee. Date Analyzed: 11/25/98
'
GC Column: DB-624 ID: 0.53 (mm}
I Soil Extract Volume : ____ (uL)
Dilution Factor: 1.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
----
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
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67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulb.de
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,l-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,l-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene · --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
5.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
1.0 u
1.0 u
1.0 u
1.0 u
0.14 J
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
2.0 u
5.0 u
1.0 u
1.0 u
(uL)
FORM 1 CLIENT SAMPLfl0069 I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-32I
ILab
Lab
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vlll5701
.Matrix: (soil/water) WATER
Sample wt/vol: 25.00 (g/mL) ML
ILevel: (low/med) LOW
% Moisture: not dee.
IGc Column: DB-624 ID: 0.53 (mm)
Extract Volume: ____ (uL)
Lab Sample ID: 9811174-01
Lab File ID: 1117401
Date Sampled: 11/20/98
Date Analyzed: 11/25/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I-
D
I
I
I
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene
~.
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
'
0.26 J
0.24 J
1.0 u
1.0 u
0.11 J
·.o.os& 1.0 u , -/fi' 0. Gt:s(o
i!l I
VOLATILE ORGANICS ANALYSIS DATA SHEET
I
I
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
TRIP B~,.,084 NK # llY.f--1 _I
~ Code: NA Batch No. : NA SAS No.: NA· SDG No.: FCX.Vlll5701
Matrix: (soil/water) WATER
Jmple wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW
I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9811157-05
Lab File ID: 1115705
Date Sampled: 11/19/98
Date Analyzed: 11/24/98
Dilution Factor: 1.0
loil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
u
I
I
g
D
0
CAS NO. COMPOUND
67-64-1---------Acetone
71-43-2---------Benzene
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-27-4--

-

-

-

-

-

-
-Bromochloromethane '·
75-27-4---------Bromodichloromethane
75-25-2---------Bromoforrn
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disull:i.ae
56-23-5---------Carbon tetrachlori.ae
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroforrn
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-D~bromo-3-chloropropane_
106-93 -4 -

-

-

-

-

-

-
-1, 2-Dibr.omoethane
95-50-1--

-

-

-

-

-

-
-1, 2-Di.chlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l 2-Dichloroethene . ' --
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone ' 75-09-2---------Methylene chloriae
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachioroethane __
FORM I VOA
Q
5.0 u
1. 0 u
1.0 u
1.0 u
1. 0 u
1.0 u
5.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1. 0 u
1.0 u
1. 0 u
1.0 u t2..
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
0.96 J
5.0 u
1.0 u
1.0 u
FORM 1 CLIENT SAMPLf>Q9_55 I VOLATILE ORGANICS ANALYSIS DATA SHEET
Jab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
TRIP ELA
NK # 1159
Lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vlll5701
latrix: (soil/water) WATER
lirample wt/vol:
l.,evel: (low/med)
25. 00 (g/mL) ML
LOW
IFCMoisture: not dee.
lie; Column: DB-624 ID: 0.53 (mm) roil Extract Volume: ____ (uL)
Lab Sample ID: 9811157-05
Lab File ID: 1115705
Date Sampled: 11/19/98
Date Analyzed: 11/24/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
u
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
-
127-18-4--------Tetrachloroethene 1. 0 u
108-88-3--------Toluene 1. 0 u
71-55-6---------1,1,1-Trichloroethane 1.0 u
79-00-5---------1,1,2-Trichloroethane 1. 0 u
79-01-6---------Trichloroethene 1.0 u
75-01-4---------Vinyl chloride 1.0 u
1330-20-7-------Xylene(total) 0,30 . ~ --~ --..... ..., -
FORM I VOA
I
I 00091
FORM 1 CLIENT SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
TRIP BLA
NK # 1158
lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vlll5701
Matrix: (soil/water} WATER Lab Sample ID: 9811174-05
lample wt/vol: 25.00 (g/mL} ML
Level: (low/med} LOW
Lab File ID:
Date Sampled:
1117405
11/20/98
I Moisture; not dee.
GC Column: DB-624 ID: 0.53 (mm}
Date Analyzed: 11/24/98
Dilution Factor: 1.0
loil Extract Volume: ____ (uL} Soil Aliquot Volume:
I
I
I
g
0
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg} UG/L
.
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfiae
56-23-5---------Carbon tetrachloriae
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene __
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chlon.ae
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
5.0
1. 0
1. 0
1. 0
1.0
1.0
5.0
1. 0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1. 0
1.0
1.0
1. 0
1.0
1.0
1.0
1. 0
5.0
1. 2
5.0
1.0
1.0
----
Q
u u u u u u u
u u u u
u u u
u u u u
u u u u
u u u
u u u
u
J u u
u
(uL}
I FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
CLIENT SAMPLQCW~2
ILab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
TRIP ELA
NK # 1158
Lab Code: NA Batch No. : NA . SAS No.: NA SDG No.: FCX.Vlll5701
IMatrix: (soil/water)
Sample wt/vol:
ILevel: (low/med)
WATER
25.00
LOW
(g/mL) ML
Lab Sample ID: 9811174-05
Lab File ID: 1117405
Date Sampled: 11/20/98
Date Analyzed: 11/24/98
Dilution Factor: 1.0 I ~ Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
lsoil Extract Volume: (uL) ----Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene
108-88-3--------Toluene ------
71-55-6---------1,l,l-Trichloroethane
79-00-5---------1,l,2-Trichloroethane ----
79-01-6---------Trichloroethene ----
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total) --------
FORM I VOA
1. 0 U
1. 0 U
1. 0 U
1. 0 U
1. 0 U
1.0U
1. 0 U
I FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
00042
CLIENT SAMPLE NO. 6!3 ~ IU-3;,:_
I Lab Name : ECKENFELDER INC. Contract: EL PASO ENERGY
EC@ W-31I
I Lab ~ode: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vlll5701
Matrix: (soil/water) WATER Lab Sample ID: 9811157-03
I Sample
Level:
wt/vol:
(low/med)
25. 00 (g/mL) ML
LOW
Lab File ID:
Date Sampled:
1115703
11/19/98
I% Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm) I Soil Extract Volume : ____ (uL)
Date Analyzed: 11/24/98
Dilution Factor: 1.0
Soil Aliquot Volume: ----
I
I
I
D
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---~-----Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene --78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
Q
5.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
5.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
0.46 J
5.0 u
1.0 u
1.0 u
(uL)
I FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
ILab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
EC@ W-31I
ILab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vlll5701
Matrix: (soil/water) WATER
lsample
Level:
wt/vol:
(low/med)
1% Moisture: not dee.
25. 00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm)
'Soil Extract Volume: ____ (uL)
Lab Sample ID: 9811157-03
Lab File ID: 1115703
Date Sampled: 11/19/98
Date Analyzed: 11/24/98
Dilution Factor: 1. 0
Soil Aliquot Volume: ----
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene 1.0 u
108-88-3--------Toluene 1.0 u
71-55-6---------1,1,1-Trichloroethane 1.0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 1.0 u
75-01-4---------Vinyl chloride 1.0 u
1330-20-7-------Xylene(total) 1.0 u
FORM I VOA
(uL)
I
lab
00063
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
HOLDING BLANK
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
liab ~ode: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vlll5701
latrix: (soil/water) WATER. Lab Sample ID: 9811157-06
'
ample
evel:
wt/vol:
(low/med)
25.00 (g/mL) ML
LOW
Lab File ID:
Date Sampled:
1115706
11/20/98
I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
Date Analyzed: 11/24/96
Dilution Factor: 1.0
loil Extract Volume: ____ (uL) Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
106-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-67-3---------Chloromethane
124-46-1--------Dibromochloromethane
96-12-6---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
76-67-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-76-6--------2-Hexanone
75-09-2---------Methylene chloride
106-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
0.22
5.0
1.0
1.0
----
u
u
u
u
u
u
u u
u u u u
u u u u
u
u
u
u
u
u
u
u u u
u
u u
J
u
u
u
(uL)
FORM 1 CLIENT SAMPLPQ9.64
VOLATILE ORGANICS ANALYSIS DATA pHEET
HOLDING BLANK
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Lab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vlll5701
liatrix: (soil/water) WATER
iii5ample wt/vol:
l.,evel: (low/med)
25. 00 (g/mL) ML
LOW
ifCMoisture: not dee.
~ Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9811157-06
Lab File ID: 1115706
Date Sampled: 11/20/98
Date Analyzed: 11/24/98
Dilution Factor: 1.0
Soil Aliquot Volume: ----roil Extract Volume: ____ (uL)
CONCENTRATION UNITS:
I
I
I
!
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
-.
127-18-4--------Tetrachloroethene 1.0 u
108-88-3--------Toluene 1.0 u
71-55-6---------1,1,1-Trichloroethane 1.0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 1.0 u
75-01-4---------Vinyl chloride 1.0 u
1330-20-7-------Xylene(total) 1. 0 u
FORM I VOA
(uL)
I FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
f.,ab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
HOLDING BLANK
Lab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vlll5701
Jatrix: (soil/water) WATER Lab Sample ID: 9811174-04
Sample wt/vol: 25.00 (g/rnL) ML Lab File ID: 1117404
level: (low/med) LOW Date Sampled: 11/23/98
I% Moisture: not dee.
llc;c Column: DB-624 ID: 0.53 (mm)
Date Analyzed: 11/24/98
Dilution Factor: 1.0
'Soil Extract Volume: ____ (uL) Soil Aliquot Volume: ___ (uL)
CONCENTRATION UNITS:
· CAS NO. COMPOUND (,ug/L or ug/Kg) UG/L Q
I
I
I
I
I
I
I
I
I
I
I
I
I
\
~
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoforrn
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulb.de
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroforrn
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene --78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
5.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u
1. 0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
5.0 u
0, 1'8' --J u
5.0 u
1. 0 u
1.0 u
I FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
CLIENT SAMPLQQ£~7
fab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
HOLDING BLANK
Lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vlll5701
latrix: (soil/water) WATER Lab Sample ID: 9811174-04
Lab File ID: 1117404
Date Sampled: 11/23/98
Date Analyzed: 11/24/98
Dilution Factor: 1.0
Sample wt/vol: 25.00 (g/mL) ML
level: (low/med) LOW
I~ Moisture: not dee.
C Column: DB-624 ID: 0.53 (mm)
Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
127-18-4--------Tetrachloroethene
108-88-3--------Toluene ------
71-55-6---------1,l,l-Trichloroethane
79-00-5~--------l,l,2-Trichloroethane ----
79-01-6---------Trichloroethene ----
75-01-4---------Vinyl chloride _______ _
1330-20-7-------Xylene(total) _______ _
FORM I VOA
l.0U
1. 0 U
1. 0 U
1. 0 U
1. 0 U
1. 0 U
1. 0 U
Q
I
I
lab
FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
CLIENT SAMPI.@0048
W-31I
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vlll5701
IMatrix: (soil/water) WATER
Sample wt/vol: 25.00 (g/mL) ML
I Level: (low/med) LOW
% Moisture: not dee.
IGc Column: DB-624 ID: 0.53 (mm)
Lab Sample ID: 9811157-04
Lab File ID: 1115704
Date Sampled: 11/19/98
Date Analyzed: 11/24/98
Dilution Factor: 1.0
'Soil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone -
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disull:iae
56-23-5---------Carbon tetrachloriae
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chloriae :;J.tf) 0-/41;
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
Q
5.0 u
1.0 u
1. 0 u
1.0 u
1. 0 u
1.0 u
5.0 u
1. 0 u
1. 0 u
1. 0 u
1.0 u
1. 0 u
1. 0 u
1.0 u
1.0 u /(
1. 0 u
1. 0 u
1. 0 u
1.0 u
1.0 u
' 1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
5.0 u ~ --v.v V
5.0 u
1. 0 u
1.0 u
I FORM 1 CLIENT SAMPL!()0049
VOLATILE ORGANICS ANALYSIS DATA SHEET
'Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
W-31I
Lab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vlll5701
IMatrix: (soil/water) WATER Lab Sample ID: 9811157-04
Sample wt/vol: 25.00 (g/mL) ML Lab File ID: 1115704
ILevel: (low/med) LOW Date Sampled: 11/19/98
% Moisture: not dee.
IGc Column: DB-624 ID: 0.53 (mm)
Date Analyzed: 11/24/98
Dilution Factor: 1.0
Extract Volume: (uL) ----Soil Aliquo·t Volume:
1soil
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I
I
I
I
I
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene -.
108-88-3--------Toluene
71-55-6---------1,1,lrTrichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
/
FORM I VOA
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
(uL)
I
I
lab
FORM 1 CLIENT SAMPLQ(M?~2
VOLATILE ORGANICS ANALYSIS DATA SHEET
W-31S
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
l·ab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vlll5701
atrix: (soil/water) WATER
lample wt/vol:
evel: (low/med)
25.00 (g/rnL) ML
LOW
Lab Sample ID: 9811157-01
Lab File ID: 1115701
Date Sampled: 11/19/98
Date Analyzed: 11/24/98
Dilution Factor: 1.0
.CMoisture: not dee.
~ Column: DB-624 ID: 0.53 (mm)
foil Extract Volume: ____ (uL) Soil Aliquot Volume: ----
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
I
I
I
I
I
I
I
I
I
I
I
I
-
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------carbon disulfide
56·23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3----·----Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-1,2-Dichloroethene
156-60-5--------trans-1,2-Dichloroethene
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-1,3-Dichloropropene
--
10061-02-6------trans-1,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1, 1, 2, 2-Tetr.achioroethane __
FORM I VOA
5.0 u
1.0 u
1. 0 u
1. 0 u
1.0 u
1. 0 u
5.0 u
1.0 u
1.0 u
1.0 u
1.0 u
0.25 J
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1. 0 u
1.0 u
5.0 u
2.0 u
5.0 u
1.0 u
1. 0 u
(uL)
I
I FORM 1 CLIENT
I VOLATILE ORGANICS ANALYSIS DATA SHEET
W-31S
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
tb Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vlll5701
Matrix: {soil/water) WATER
tmple wt/vol: 25. 00 {g/mL) ML
Level: {low/med) LOW
I Moisture: not dee.
GC Column: DB-624 ID: 0.53 {mm)
Lab Sample ID: 9811157-01
Lab File ID: 1115701
Date Sampled: 11/19/98
Date Analyzed: 11/24/98
Dilution Factor: 1.0
Soil Aliquot Volume: loil Extract Volume : ____ {uL) ----
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
127-18-4--------Tetrachloroethene
CONCENTRATION UNITS:
{ug/L or ug/Kg) UG/L
1. 0
108-88-3--------Toluene o.oc.'ff, -

.

:
71-55-6---------1,1,1-Trichloroethane 1. 0
79-00-5---------1,1,2-Trichloroethane 1.0
79-01-6---------Trichloroethene 1. 0
75-01-4---------Vinyl chloride 1.0
1330-20-7-------Xylene{total) 1.0
FORM I VOA
Q
-
u -::r 7
u u u u u
(uL)
I FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
.b Name: ECKENFELDER INC. Contract: EL PASO ENERGY
W-31S DUPE
Lab Code: NA Batch No.: NA SAS No.: NA SDG No.: FCX.Vll15701
Jtrix: (soil/water) WATER Lab Sample ID: 9811157-02
jample wt/vol:
evel: (low/med)
25.00 (g/mL) ML
LOW
Lab File ID: 1115702
Date Sampled: 11/19/98
Date Analyzed: 11/25/98
Dilution Factor: 1.0 I• Moisture: not dee.
C Column: DB-624 ID: 0.53 (mm)
loil Extract Volume : _____ (uL) Soil Aliquot Volume: ----
CONCENTRATION UNITS.:
I
I
I
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
I
I
I
I
I
I
I
I
I
I
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-1,2-Dichloroethene
156-60-5--------trans-1,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-1,3-Dichloropropene
10061-02-6------trans-1,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
5.0 u
1.0 u
1. 0 u
1.0 u
1. 0 u
1.0 u
5.0 u
1.0 u
1.0 u
1.0 u
1.0 u
0.29 J
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1. 0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
5.0 u
2.0 u
5.0 u
1.0 u
1.0 u
{uL)
FORM l
VOLATILE ORGANICS ANALYSIS DATA SHEET
CLIENT SAMPL~(!J()33
W-3lS DUPE
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vlll5701
[
trix: (soil/water)
mple wt/vol:
tvel: (low/med)
% Moisture: not dee.
le Column: DB-624
WATER
25.00 (g/mL) ML
LOW
ID: 0.53 (mm)
Lab Sample ID: 98lll57-02
Lab File ID: lll5702
Soil
' I
Extract Volume: (uL) -----
Date Sampled: 11/19/98
Date Analyzed: 11/25/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (UL)
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
J') I.
)p"~v'if -'"l,,,,r
--------------------------,--------,----'i·
127-18-4--------Tetrachloroethene ,
108-88-3--------Toluene ------
71-55-6---------1,l,l-Trichloroethane
79-00-5---------l,l,2-Trichloroethane ___ _
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride-------
1330-20-7-------Xylene(total) _______ _
FORM I VOA
\
l.O U
1. 0 U
l.0U
1. 0 U
1. 0 U
l.0U
1. 0 U
I
I FORM 1 CLIENT SAMPL2~?8
VOLATILE ORGANICS ANALYSIS DATA SHEET
ILab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
WOOTEN WELL
I-.Lab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.V1115701
Matrix: (soil/water) WATER
I Sample wt/vol:
Level: (low/med)
25.00 (g/mL) ML
LOW
Lab
Lab
Date
Date
Sample ID: 9811174-02
File ID: 1117402
Sampled: 11/20/98
Analyzed: 11/25/98
I.% Moisture: not dee.
. GC Column: DB-624 ID: 0.53 (mm) Dilution Factor: 1.0
'Soil
I
1·
I
I
I
I
I
I
I
I
I
I
Extract Volume: ____ (uL) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
~
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulriae
56-23-5---------Carbon tetrachloriae
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93~4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-1,2-Dichloroethene
156-60-5--------trans~l,2-Dichloroethene __
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-1,3-Dichloropropene
10061-02-6------trans-1,3-Dichloropropene __ ' 100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chloriae
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM .I VOA
5.0
1.0
1.0
1. 0
1.0
1.0
5.0
1.0
1. 0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1. 0
1. 0
1. 0
1. 0
1. 0
1.0
1. 0
1.0
1. 0
1.0
5.0
2.0
5.0
1.0
1.0
____ (uL)
Q
u
u u u u u u
u u
u u u
u u u u u u
u u u u
u
u u u
u u u
u u u
u
VOLATILE ORGANIC~ ANALY~~~ LJAlA un~~.
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
WOOTEN wR2°l 9
SDG No.: FCX.Vlll5701
Batch No.: NA lab Code: NA
Matrix: (soil/water)
SAS No.: NA
WATER
fample wt/vol: 25.00 (g/mL) ML
Level: (low/med) LOW I Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
loil Extract Volume : ____ (uL)
Lab Sample ID: 9811174-02
Lab File ID: 1117402
\
Date Sampled: 11/20/98
Date Analyzed: 11/25/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene
1.0 u
108-88-3--------Toluene
1.0 u
71-55-6---------1,1,1-Trichloroethane
1.0 u
79-00-5---------1,1,2-Trichloroethane
1.0 u
79-01-6---------Trichloroethene
1.0 u
75-01-4---------Vinyl chloride 1.0 u
1330-20-7-------Xylene(total) 1.0 u
FORM I VOA
I
I FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Code: NA Batch No. : NA SAS No.: NA
00082
CLIENT SAMPLE NO.
HINSON WELL
SDG No.: FCX.Vlll5701
Matrix: (soii/water) WATER Lab Sample ID: 9811174-03
Lab File ID: 1117403
Date Sampled: 11/20/98
Date Analyzed: 11/25/98
Dilution Factor: 1.0
f.mple wt/vol: 25.00 (g/rnL) ML
Level: (low/med) LOW
I I Moisture: not dee.
GC Column: DB-624 ID: 0. 53 (mm)
Extract Volume: (uL) -----Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I·
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoforrn
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-D~bromo-3-chloropropane_
106-93-4--------1,2-Dibromoethane
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene __
100-41-4--------Ethylbenzene
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
5.0
1. 0
1. 0
1. 0
1. 0
1.0
5.0
1.0
1.0
1. 0
1. 0
1.0
1. 0
1. 0
1.0
1.0
1.0
1. 0
1.0
1.0
1. 0
1.0
1. 0
1.0.
1.0
1.0
1.0
1.0
5.0
2.0
5.0
1.0
1.0
____ (uL)
Q
u u u
u u u
u u u
u
u u u u u (.'...__
u u u u
u u
u u u u u u
u u u
u u
u
I
I 00083
FORM 1 CLIENT SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
HINSON WELL
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
tab Code: NA Batch No. : NA SAS No.: NA SDG No.: FCX.Vlll5701
· Matrix: (soil/water) WATER
'Sample wt/vol:
Level: (low/med)
25.00 (g/mL) ML
LOW
1% Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm)
'Soil Extract Volume : ____ (uL)
Lab Sample ID: 9811174-03
Lab File ID:
Date Sampled:
1117403
11/20/98
Date Analyzed: 11/25/98
Dilution Factor: 1.0
Soil Aliquot Volume: ----
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I
I
I
I
I
I
I
I
I
-
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
(uL)
FORM 1
0014ts
CLIENT SAMPLE NO. I PESTICIDE ORGANICS ANALYSIS DATA SHEET
W-31S
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
IT ab ~ode: NA Batch No. : NA SAS No.: NA SDG No.: ELP.Plll57-0l
atrix: (soil/water) WATER
ramp le wt/vol:
-. Moisture:
1000 (g/mL) ML
decanted: (Y/N)
fxtraction: (SepF/Cont/Sonc/Soxh) SEPF
Concentrated Extract Volume: 2 (mL)
tnjection Volume: 1. 0 (uL)
Lab Sample ID: 9811157-.01
Lab File ID: 022F0101
Date Sampled: 11/19/98
Date Extracted: 11/24/98
Date Analyzed: 12/22/98
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N
I
pH: NA Sulfur Cleanup: (Y/N) N
CONCENTRATION UNITS:
I:
I
I
I
I'
I
I
I
I
I
I
I
CAS NO. COMPOUND (u_g/L or ug/Kg) UG/L Q
309-00-2--------Aldrin 0.010 u
319-84-6--------alpha-BHC 0.010 u
5103-71-9-------alpha-Chlordane 0.010 u
319-85-7--------beta-BHC 0.010 u
72-54-8---------4,4'-DDD 0.020 u
72-55-9---------4,4'-DDE 0.020 u
50-29-3---------4,4'-DDT 0.020 u
60-57-1---------Dieldrin 0.020 u
319-86-8--------delta-BHC 0.010 u
959-98-8--------Endosulfan I 0.010 u
33213-65-9------Endosulfan II 0.020 u
1031-07-8-------Endosulfan suI:Eate 0.020 u
72-20-8---------Endrin 0.020 u
7421-36-3-------Endrin aicteFiyde 0.020 u
53494-70-5------Endrin ketone 0.020 u
58-89-9---------gamma-BHC (Lindanej 0.010 u
5103-74-2-------gamma-Chlordane 0.010 u
76-44-8---------Heptachlor 0.010 u
1024-57-3-------Heptachlor epoxide 0.010 u
72-43-5---------Methoxychlor 0.10 u
8001-35-2-------Toxaphene 1.0 u
12674-11-2------Aroclor-1016 0.20 u
11104-28-2------Aroclor-1221 0.40 u
1114-16-5-------Aroclor-1232 0.20 u
53469-21-9------Aroclor-1242 0.20 u
12672-29-6------Aroclor-1248 0.20 u
11097-69-1------Aroclor-1254 0.20 u
11096-82-5------Aroclor-1260 0.20 u
FORM I PEST
I
lab
FORM 1
PESTICIDE ORGANICS ANALYSIS DATA SHEET
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
00155
CLIENT SAMPLE NO.
W-31S DUPE
lab ~ode: NA Batch No. : NA
atrix: (soil/water) WATER
SAS No.: NA SDG No.: ELP.P11157-0l
Lab Sample ID: 9811157-02
Lab File ID: 023F0101
D~te Sampled: 11/19/98
Date Extracted: 11/24/98
Date Analyzed: 12/22/98
Dilution Factor: 1.0
'ample wt/vol:
-c;
1
Moisture:
1000 (g/mL) ML
decanted: ( Y /N)
fxtraction: (SepF/Cont/Sonc/Soxh) SEPF
Concentrated Extract Volume: 2 (mL)
Injection Volume: 1. 0 (uL)
GPC Cleanup: (Y/N) N pH: NA Sulfur Cleanup: (Y/N) N
I
I
D ,,
I
I'
I
'I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
309-00-2--------Aldrin
319-84-6--------alpha-~B~H~c-------------
5103-71-9-------alpha-Chlordane ______ _
319-85-7--------beta-BHC 72-54-8---------4,4'-DDD __________ _
72-55-9---------4,4'-DDE __________ _
50-29-3---------4,4'-DDT 60-57-1---------Dieldrin __________ _
319-86-8--------delta-BHC 959-98-8--------Endosulfa-n--.I ________ _
33213-65-9------Endosulfan I~I--------
1031-07-8-------Endosulfan sulfate
72-20-8---------Endrin -----
7421-36-3-------Endrin-a~r-are~h-y-dTe,--------
53494-70-5------Endrin ketone
58-89-9---------gamma-BHC (Li-n~a~a_n_e~)-----
5103-74-2-------gamma-Chlordane ______ _
76-44-8---------Heptachlor
1024-57-3-------Heptachlor_e_p_o_x_ird~e------
72-43-5---------Methoxychlor ________ _
8001-35-2-------Toxaphene
12674-ll-2------Aroclor-1~0~1~6---------
11104-28-2------Aroclor-1221
1114-16-5-------Aroclor-1232 ________ _
53469-21-9------Aroclor-1242
12672-29-6------Aroclor-1248 ________ _
11097-69-1------Aroclor-1254
11096-82-5------Aroclor-1260 ________ _
FORM I PEST
0.010
0.010
0.0024
0.010
0.020
0.020
0.020
0.020
0.0037
0.010
0.020
0.020
0.020
0.020
0.020
0.010
0.010
0.010
0.010
0.10
1. 0
0.20
0.40
0.20
0.20
0.20
0.20
0.20
u u
J u u u u u
JP u u u u u u u u u u u u u u u u u u u
Q
I FORM 1
00162
CLIENT SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EB@ W-31I
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Ji,ab ~ode: NA Batch No. : NA
'tiatr1.x: (soil/water) WATER
SAS No.: NA SDG No.: ELP.Plll57-01
Lab Sample ID: 9811157-03
Lab File ID: 024F0101
Date Sampled: 11/19/98
Date Extracted: 11/24/98
Date Analyzed: 12/22/98
Dilution Factor: 1.0
'ample wt/vol:
% Moisture:
1000 (g/mL) ML
decanted: (Y /N)
J:xtraction: (SepF/Cont/Sonc/Soxh) SEPF
Concentrated Extract Volume: 2(mL)
lrnjection Volume: l.0(uL)
GPC
I ,.
I
I
I ,, ,,
I
I
I
I
I
I
I
Cleanup: (Y/N) N
CAS NO.
pH: NA
COMPOUND
Sulfur Cleanup:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
309-00-2--------Aldrin
319-84-6--------alpha-~B~H~C.-----------
5103-71-9-------alpha-Chlordane
319-85-7----~---beta-BHC -------
72-54-8---------4,4'-DDD 72-55-9---------4,4'-DDE __________ _
50-29-3---------4,4'-DDT 60-57-1---------Dieldrin __________ _
319-86-8--------delta-BHC
959-98-8--------Endosulfa-n~I---------
33213-65-9------Endosulfan II
•1031-07-8-------Endosulfan su-l~f_a_t_e _____ _
,.72-20-8--

-

-

-

-

-

-
-Endrin 7421-36-3-------Endrin-a~r-are,h_y_d_e _______ _
53494-70-5------Endrin ketone
58-89-9---------gamma-BHC (Li_n_d_a_n_e~)~----
5103-74-2-------gamma-Chlordane -------76-44-8---------Heptachlor
1024-57-3-------Heptachlor_e_p_o_x_i_d~e------
72-43-5---------Methoxychlor ________ _
8001-35-2-------Toxaphene
12674-ll-2------Aroclor-1=0=1~6---------
11104-28-2------Aroclor-1221 1114-16-5-------Aroclor-1232 ________ _
53469-21-9------Aroclor-1242 ________ _
12672-29-6------Aroclor-1248 11097-69-1------Aroclor-1254 ________ _
11096-82-5------Aroclor-1260 ---------
FORM I PEST
(Y/N) N
0.010 U
0.010 U
0.010 U
0.010 U
0.020 U
0.020 U
0.020 U
0.020 U
0.010 U
0.010 U
0.020 U
0.020 U
0.020 U
0.020 U
0.020 U
0.010 U
0.010 U
0.010 U
0.010 U
0.10 U
1. 0 U
0.20 U
0.40 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
Q
00167
I. FORM 1 CLIENT SAMPLE NO,
PESTICIDE ORGANICS ANALYSIS DATA SHEET
,,ab Name: ECKENFELDER INC, Contract: EL PASO ENERGY
W-31 I
llfab ~ode: NA Batch No, : NA SAS No,: NA SDG No,: ELP,Plll57-0l
'1atrix: (soil/water) WATER
l ample wt/vol:
· -6 Moisture:
1000 (g/mL) ML
decanted: (Y /N)
fxtraction:
•✓concentrated
(SepF/Cont/Sonc/Soxh) SEPF
Extract Volume: 2 (mL)
.tnjection Volume: l, O (uL)
Lab Sample ID: 9811157-04
Lab File ID: 025F0101
Date Sampled: 11/19/98
Date Extracted: 11/24/98
Date Analyzed: 12/22/98
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: NA
I
Sulfur Cleanup: (Y/N) N
CONCENTRATION UNITS:
I
I
I
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
309-00-2--------Aldrin
319-84-6--------alpha-BHC
5103-71-9-------alpha-Chlordane
319-85-7--------beta-BHC
72-54-8---------4,4'-DDD
72-55-9---------4,4'-DDE
50-29-3---------4,4'-DDT
60-57-1---------Dieldrin
319-86-8--------delta-BHC
959-98-8--------Endosulfan I
33213-65-9------Endosulfan II
1031-07-8-------Endosulfan suif,ate
72-20-8---------Endrin
7421-36-3-------Endrin aiclenycle
53494-70-5------Endrin ketone
58-89-9---------gamma-BHC (Lindane)
5103-74-2-------gamma-Chlordane
76-44-8---------Heptachlor :
1024-57-3-------Heptachlor epoxide
72-43-5---------Methoxychlor
8001-35-2-------Toxaphene
12674-11-2------Aroclor-1016
11104-28-2------Aroclor-1221
1114-16-5-------Aroclor-1232
534~9-21-9------Aroclor-1242
12672-29-6------Aroclor-1248
11097-69-1------Aroclor-1254
11096-82-5------Aroclor-1260
FORM I PEST
Q
0.010 u
0.010 u
0.010 u
0.010 u
0.020 u
0.020 u
0.020 u
0.020 u
0.010 u
0.010 u
0.020 u
0.020 u
0.020 u
0.020 u
0.020 u
0.010 u
0.010 u
0.010 u
0.010 u
0.10 u
1.0 u
0.20 u
0. 40 u
0.20 u
0.20 u
0.20 u
0.20 u
0.20 u
ljj
00174
I. FORM 1 CLIENT SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
Jab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
W-32I
Lab Code: NA Batch No.: NA SAS No.: NA SDG No.: ELP.Plll57-01
lqatrix: (soil/water) WATER
liifamp~e wt/vol:
•~ Moisture: . __ _
1000 (g/mL).ML
decanted: (Y/N)
■Extraction:
econcentrated
(SepF/Cont/Sonc/Soxh) SEPF
Extract Volume: 2 (mL)
1
1Injection Volume:
GPC Cleanup: (Y/N) N
1. 0 (uL)
pH: NA
Lab Sample ID: 9811174-01
Lab File ID: 026F0101
Date Sampled: 11/20/98
Date Extracted: 11/24/98
Date Analyzed: 12/22/98
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N • CAS NO. '··
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
g,
.. Ji, U,
g
I
V
I:
·1
-·I \I ,,
I
I
I:
309-00-2--------Aldrin
319-84-6--------alpha-BHC
5103-71-9-------alpha-Chlordane
319-85-7--------beta-BHC
72-54-8---------4,4'-DDD
72-55-9---------4,4'-DDE
50-29-3---------4,4'-DDT
60-57-1---------Dieldrin
319-86-8--------delta-BHC
959-98-8--------Endosulfan I
33213-65-9------Endosulfan II
1031-07-8-------Endosulfan suil:ate
72-20-8---------Endrin
7421-36-3-------Endrin aiclenyde
53494-70-5------Endrin ketone
58-89-9---------gamma-BHC (Lindane)
5103-74-2-------gamma-Chlordane
76-44-8---------Heptachlor --·
1024-57-3-------Heptachlor epoxide
72-43-5---------Methoxychlor
8001-35-2-------Toxaphene
12674-11-2------Aroclor-1016
11104-28-2------Ar9clor-1221
1114-16-5-------Aroclor-1232
53469-21-9------Aroclor-1242
12672-29-6------Aroclor-1248
11097-69-1------Aroclor-1254
11096-82-5------Aroclor-1260
FORM I PEST
0.0055 JP
0.0027 JP
0.010 u
0.010 u
0.0096 JP
0.020 u
0.020 u
0.015 J
0.079 p
0.0055 JP
0.020 u
0.020 u
0.020 u
0.020 u
0.020 u
0.010 u
0.0020 JP
0.014 p
0.0060 JP
0.10 u
1. 0 u
0.20 u
0.40 u
0.20 u
0.20 u
0.20 u
0.20 u
0.20 u
:r
T
-,-
FORM 1
00181
CLIENT SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
WOOTEN WELL
Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Lab Code: NA Batch No. : NA SAS No.: NA SDG No.: ELP.Plll57-01
latrix: (soil/water) WATER
lil'amp~e wt/vol:
a Moisture:
1000 (g/mL) ML
decanted: (Y /N) ---
lxtraction:
oncentrated
(SepF/Cont/Sonc/Soxh) SEPF
Extract Volume: 2 (mL)
Injection Volume: 1.0 (uL)
GPC Cleanup: (Y/N) N pH: NA
Lab Sample ID: 9811174-02
Lab File ID: 027F0101
Date Sampled: 11/20/98
Date Extracted: 11/24/98
Date Analyzed: 12/22/98
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N
I
:I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
-
I
I
I' '
I
I
I ,,
I
309-00-2--------Aldrin
319-84-6--------alpha-BHC
5103-71-9-------alpha-Chlordane
319-85-7--------beta-BHC
72-54-8---------4,4'-DDD
72-55-9---------4,4'-DDE
50-29-3---------4,4'-DDT
60-57-1---------Dieldrin
319-86-8--------delta-BHC
959-98-8--------Endosulfan I
33213-65-9------Endosulfan II
1031-07-8-------Endosulfan sulfate
72-20-8---------Endrin
7421-36-3-------Endrin aideFiyde
53494-70-5------Endrin ketone
58-89-9---------gamma-BHC (Lindane)
5103-74-2-------gamma-Chlordane
76-44-8---------Heptachlor
1024-57-3-------Heptachlor epox1.de
72-43-5---------Methoxychlor
8001-35-2-------Toxaphene
12674-11-2------Aroclor-1016
11104-28-2------Aroclor-1221
1114-16-5-------Aroclor-1232
53469-21-9------Aroclor-1242
12672-29-6------Aroclor-1248
11097-69-1------Aroclor-1254
11096-82-5------Aroclor-1260
FORM I PEST
0.010 u
0.010 u
0.010 u
0.010 u
0.020 u
0.020 u
0.020 u
0.020 u
0.010 u
0.010 u
0.020 u
0.020 u
0.020 u
0.020 u
0.020 u
0.010 u
0.010 u
0.010 u
0.010 u
0.10 u
1.0 u
0.20 u
0.40 u
0.20 u
0.20 u
0.20 u
0.20 u
0.20 u
u-:r
I
00188
FORM 1 CLIENT SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
HINSON WELL
iii'ab Code: NA Batch No. : NA SAS No.: NA SDG No.: ELP.Plll57-0l
latrix: (soil/water) WATER
liample wt/vol:
Ill Moisture: ---
1000 (g/mL) ML
decanted: (Y/N)
1xtraction:
'-oncentrated
(SepF/Cont/Sonc/Soxh) SEPF
Extract Volume: 2 (mL)
lnj ection Volume: 1. 0 (uL)
Lab Sample ID: 9811174-03
Lab File ID: 028F0101
Date Sampled: 11/20/98
Date Extracted: 11/24/98
Date Analyzed: 12/22/98
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: NA Sulfur Cleanup: (Y/N) N
CONCENTRATION UNITS: I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
309-00-2--------Aldrin
319-84-6--------alpha-~B~H=cc------------
5103-71-9-------alpha-Chlordane
319-85-7--------beta-BHC -------
72-54-8---------4,4'-DDD 72-55-9---------4,4'-DDE __________ _
50-29-3---------4,4'-DDT 60-57-1---------Dieldrin __________ _
319-86-8--------delta-BHC 959-98-8----~---Endosulfa_n_I ________ _
33213-65-9------Endosulfan II
1031-07-8-------Endosulfan su~l7f-a~t_e _____ _
72-20-8---------Endrin
7421-36-3-------Endrin-a~l-d~e~h-y-d~e--------
53494-70-5------Endrin ketone
58-89-9---------gamma-BHC (Li_n_d_a_n_e_) ____ _
5103-74-2-------gamma-Chlordane ______ _
76-44-8---------Heptachlor
1024-57-3-------Heptachlor_e_p_o_x_i_d~e------
72-43-5---------Methoxychlor ________ _
8001-35-2-------Toxaphene
12674-ll-2------Aroclor-1~0~1~6---------
11104-28-2------Aroclor-1221 1114-16-5-------Aroclor-1232 ________ _
53469-21-9------Aroclor-1242 12672-29-6------Aroclor-1248 ________ _
11097-69-1------Aroclor-1254 11096-82-5------Aroclor-1260 ________ _
FORM I PEST
0.010 U
0.010 U
0.010 U
0.010 U
0.020 U
0.020 U
0.020 U
0.020 U
0.010 U
0.010 U
0.020 U
0.020 U
0.020 U
0.020 U
0.020 U
0.010 U
0.010 U
0.010 U
0.010 U
0.10 U
1. 0 U
0.20 U
0.40 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
Q
V-.1
I
I
I
I
I
I
I
I
I
I
D
I
I
I
I-
I
I
I
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SnEET
Lab Name: ECKENFELDER INC. Contrac:: El Paso Energy -------------------
Lab Code: Case No.: SAS No.: -----------------
Matrix· (soil/water I: WATER Lab Sample Iw: 9809144-01 ---------
Level (low/med): Date Received: 09/24/98 ---------
% Solids: 0.0
Concentration Units (ug/L or mg/kg dry weight): ug/L
' ' !CAS No. Analyte Concentration C Q
7429-90-5 Aluminum 188 B
7440-36-0 Antimony 1. 2 u
,7440-38-2 Arsenic 1. 3 u
:7440-39-3 Barium 543
:7440-41-7 Beryllium 0.10 u
:7440-43-9 Cadmium 0.19 B
:7440-70-2 Calcium 105000
!7440-47-3 Chromium 5.6 B
:7440-48-4 Cobalt 0.73 B
:7440-50-8 Copper 4. 7 a
!7439-89-6 Iron 40.6 8
:7439-92-1 Lead 2.0 8
:7439-95-4 Magnesium 230 B
:7 439-96-5 Manganese 0.88 8
!7439-97-6 Mercury 0 .13 8
!7440-02-0 Nickel 5.2 8
:7440-09-7 Potassium 212 B
:7782-4 9-2 Selenium 1. 7 B
:7440-22-4 Silver 0.10. u
:7440-23-5 Sodium 109000
:7440-28-0 Thallium 1. 4 u
:7440-62-2 Vanadium 4. 8 8
:7440-66-6 Zinc 18.4 B
' Cyanide ' '
Color Before: Clarity Before: Texture:
Color After: Clarity After: Artifacts:
Comments:
pl FORM I -IN
00006
EPA SAMPLE NO.
M
p
p
p
p
p
p
p
p
p
p
p
p
p
p
p
p
p
p
p
p
p
p
p
W-20D
SDG No.: 98P01(ICP)
98P02(Hg)
I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
W-20D
I Lab Code : NA
Matrix: (soil/water) WATER
Batch No. : NA SAS No.: NA SDG No.: ELPASO.V09144
Lab Sample ID: 9809144-01
Lab File ID: 0914401
Date Sampled: 09/23/98
Date Analyzed: 10/01/98
Dilution Factor: 1.0
I Sample wt/vol:
Level: (low/med) I % Moisture: not dee.
GC Column: DB-624
25.00 (g/mL) ML
LOW
ID: 0.53 (mm) I Soil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (uL)
CONCENTRATION UNITS:
I CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
I
I
I
u
I
I
I
I
I
I
I
I
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1;1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
22
1. 0 u
1. 0 u
1.0 u
1.0 u
1.0 u
5.0 u
1.0 u
1.0 u
1.0 u
1.0 u
0.50 J
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1. 0 u
1. 0 u
1.0 u
1.0 u
9.4
1.0 u
2.8
1.0 u
1.0 u
1.0 u
5.0 u
0.58 J
5.0 u
1.0 u
1.0 u
I FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
CLIENT SAMPLE NO.
I Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
W-20D
I Lab Code : NA
Matrix: (soil/water) WATER
Batch No. : NA SAS No.: NA SDG No.: ELPASO.V09144
Lab Sample ID: 9809144-01
Lab File ID: 0914401
Date Sampled: 09/23/98
Date Analyzed: 10/01/98
Dilution Factor: 1.0
I
I
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
25.00 (g/mL) ML
LOW
GC Column: DB-624 ID: 0.53 (mm) I Soil Extract Volume: ____ (uL) Soil Aliquot Volume:
I
I
I
I
I
I
I
n
D
I
I
CAS NO. COMPOUND
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
35
0.88
1.0
1. 0
4.9
1.0
1.0
____ (uL)
Q
E
J u u
u u
I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name : ECKENFELDER INC. Contract: EL PASO ENERGY
W-20D
I Lab Code: NA Batch No. : NA SAS No.: NA SDG No.: ELPASO.V09144
Matrix: (soil/water) WATER
I Sample wt/vol:
Level: (low/med)
25.00 (g/mL) ML
LOW
Lab Sample ID: 9809144-01
Lab File ID: 0914401D
Date Sampled: 09/23/98
Date Analyzed: 10/01/98
Dilution Factor: 25.0 I % Moisture: not dee.
GC Column: DB-624 ID: 0.53 (mm) I Soil. Extract Volume: ____ (uL) Soil Aliquot Volume: ----
CONCENTRATION UNITS:
I CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
I
I
I
I
I
m
D
D
I
I
I
67-64-1---------Acetone
71-43-2---------Benzene
75-27-4---------Bromochloromethane
75-27-4---------Bromodichloromethane
75-25-2---------Bromoform
74-83-9---------Bromomethane
78-93-3---------2-Butanone
75-15-0---------Carbon disulfide
56-23-5---------Carbon tetrachloride
108-90-7--------Chlorobenzene
75-00-3---------Chloroethane
67-66-3---------Chloroform
74-87-3---------Chloromethane
124-48-1--------Dibromochloromethane
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
75-35-4---------1,1-Dichloroethene
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-l,2-Dichloroethene
78-87-5---------1,2-Dichloropropane --
10061-01-5------cis-l,3-Dichloropropene
10061-02-6------trans-l,3-Dichloropropene
100-41-4--------Ethylbenzene --
591-78-6--------2-Hexanone
75-09-2---------Methylene chloride
108-10-1--------4-Methyl-2-pentanone
100-42-5--------Styrene
79-34-5---------1,1,2,2-Tetrachloroethane --
FORM I VOA
120 UD
25 UD
25 UD
25 UD
25 UD
25 UD
120 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
25 UD
7.4 JD
25 UD
25 UD
25 UD
25 UD
25 UD
120 UD
50 UD
120 UD
25 UD
25 UD
(uL)
I FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
CLIENT SAMPLE NO.
I Lab Name: ECKENFELDER INC.
W-20D
Contract: EL PASO ENERGY
I Lab Code : NA
Matrix: (soil/water) WATER
Batch No.: NA SAS No.: NA SDG No.: ELPASO.V09144
Lab Sample ID: 9809144-01
Lab File ID: 0914401D
Date Sampled: 09/23/98
Date Analyzed: 10/01/98
Dilution Factor: 25.0
I
I
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB-624
25. 00 (g/mL) ML
LOW
ID: 0.53 (mm) I Soil Extract Volume : ____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
D
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene 34 D
108-88-3--------Toluene 25 UD
71-55-6---------1,1,1-Trichloroethane 25 UD
79-00-5---------1,1,2-Trichloroethane 25 UD
79-01-6---------Trichloroethene 25 UD
75-01-4---------Vinyl chloride 25 UD
1330-20-7-------Xylene(total) 25 UD
FORM I VOA
I
I
I
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
VlBLKl00l
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Lab Code: NA Batch No.: NA SAS No.: NA SDG No.: ELPASO.V09144
Matrix: (soil/water) WATER Lab Sample ID: VlBLKl00l
I Sample wt/vol:
Level : (low/med)
25.00 (g/mL) ML
LOW
Lab File ID: VlBLK0l
Date Sampled:
I % Moisture: not dee.
GC Column: DB-624 ID: 0. 53 (mm)
Date Analyzed: 10/01/98
Dilution Factor: 1.0 I Soil Extract Volume : _____ (uL) Soil Aliquot Volume: ----
I
I
I
I
g
D
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
67-64-1---------Acetone 5.0 u
71-43-2---------Benzene 1.0 u
75-27-4---------Bromochloromethane 1. 0 u
75-27-4---------Bromodichloromethane 1. 0 u
75-25-2---------Bromoform 1.0 u
74-83-9---------Bromomethane 1.0 u
78-93-3---------2-Butanone 5.0 u
75-15-0---------Carbon disulfide 1.0 u
56-23-5---------Carbon tetrachloride 1.0 u
108-90-7--------Chlorobenzene 1.0 u
75-00-3---------Chloroethane 1.0 u
67-66-3---------Chloroform 1.0 u
74-87-3---------Chloromethane 1.0 u
124-48-1--------Dibromochloromethane 1.0 u
96-12-8---------1,2-Dibromo-3-chloropropane 1. 0 u
106-93-4--------1,2-Dibromoethane -1.0 u
95-50-1---------1,2-Dichlorobenzene 1.0 u
541-73-1--------1,3-Dichlorobenzene 1.0 u
106-46-7--------1,4-Dichlorobenzene 1.0 u
75-34-3---------1,1-Dichloroethane 1.0 u
107-06-2--------1,2-Dichloroethahe 1.0 u
75-35-4---------1,1-Dichloroethene 1.0 u
156-59-2--------cis-1,2-Dichloroethene 1.0 u
156-60-5--------trans-l,2-Dichloroethene 1.0 u
78-87-5---------1,2-Dichloropropane --1.0 u
10061-01-5------cis-1,3-Dichloropropene 1.0 u
10061-02-6------trans-1,3-Dichloropropene 1. 0 u
100-41-4--------Ethylbenzene --1.0 u
591-78-6--------2-Hexanone 5.0 u
75-09-2---------Methylene chloride 2.0 u
108-10-1--------4-Methyl-2-pentanone 5.0 u
100-42-5--------Styrene 1. 0 u
79-34-5---------1,1,2,2-Tetrachloroethane 1.0 u --
FORM I VOA
(uL)
I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name : ECKENFELDER INC. Contract: EL PASO ENERGY
VlBLKl00l
I Lab Code : NA Batch No. : NA SAS No.: NA SDG No.: ELPASO.V09144
Matrix: (soil/water) WATER
I Sample wt/vol :
Level: (low/med)
I % Moisture: not dee.
GC Column: DB-624
25. 00 (g/mL) ML
LOW
ID: 0.53 (mm) I Soil Extract Volume: ____ (uL)
Lab Sample ID: VlBLKl00l
Lab File ID: VlBLK0l
Date Sampled:
Date Analyzed: 10/01/98
Dilution Factor: 1.0
Soil Aliquot Volume: ----
CONCENTRATION UNITS:
I
I
I
I
g
D
I
I
I
I
I
I
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
127-18-4--------Tetrachloroethene 1.0 u
108-88-3--------Toluene 1.0 u
71-55-6---------1,1,1-Trichloroethane 1.0 u
79-00-5---------1,1,2-Trichloroethane 1.0 u
79-01-6---------Trichloroethene 1. 0 u
75-01-4---------Vinyl chloride 1.0 u
1330-20-7-------Xylene(total) 1.0 u
FORM I VOA
(uL)
I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
TRIP BLA
NK #1110
I Lab Code : NA Batch No. : NA
Matrix: (soil/water) WATER
SAS No.: NA SDG No.: ELPASO.V09144
Lab Sample ID: 9809144-02
Lab File ID: 0914402
Date Sampled: 09/23/98
Date Analyzed: 10/01/98
Dilution Factor: 1.0
I
I
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB-624
25.00 (g/mL) ML
LOW
ID: 0.53 (mm) I Soil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (uL)
I
I
I
m
I
0
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
67-64-1---------Acetone 71-43-2---------Benzene ___________ _
75-27-4---------Bromochloromethane 75-27-4---------Bromodichlorometha_n_e ____ _
75-25-2---------Bromoform 74-83-9---------Bromometh_a_n_e ________ _
78-93-3---------2-Butanone
75-15-0---------Carbon dis-u~l~f~i-a~e-------
56-23-5---------carbon tetrachloride
108-90-7--------Chlorobenzene -----
75-00-3---------Chloroethane
67-66-3---------Chloroform ---------
74-87-3---------Chloromethane 124-48-1--------Dibromochloro_m_e~t~h-a_n_e ____ _
96-12-8---------1,2-Dibromo-3-chloropropane
106-93-4--------1,2-Dibromoethane -
95-50-1---------1,2-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene ____ _
106-46-7--------1,4-Dichlorobenzene
75-34-3---------1,1-Dichloroethane -----
107-06-2--------1,2-Dichloroethane 75-35-4---------1,1-Dichloroethene _____ _
156-59-2--------cis-l,2-Dichloroethene
156-60-5--------trans-1,2-Dichloroethe~n~e-.--
78-87-5---------1,2-Dichloropropane ___ ====
10061-01-5------cis-1,3-Dichloropropene
10061-02-6------trans-1,3-Dichloroprope_n_e __
100-41-4--------Ethylbenzene _______ ===
591-78-6--------2-Hexanone 75-09-2---------Methylene -cTh~l-o_r_i_d~e------
108-10-1--------4-Methyl-2-pentanone ____ _
100-42-5--------Styrene ____ ~---~---
79-34-5---------1,1,2,2-Tetrachloroethane __
FORM I VOA
5.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
5.0 U
1. 0 U
1. 0 U
1. 0 U
1.0 U
1.0 U
1. 0 U
1.0 U
1.0U
1. 0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0U
1.0 U
1. 0 U
1. 0 U
1. 0 U
1.0 U
1.0U
5. 0 U
0.33 J
5. 0 U
1. 0 U
1.0 U
I FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
TRIP BLA
NK #1110
I Lab Code : NA Batch No. : NA SAS No.: NA SDG No.: ELPASO.V09144
Matrix: (soil/water) WATER
I Sample wt/vol:
Level: (low/med)
I % Moisture: not dee.
GC Column: DB-624
25.00 (g/mL) ML
LOW
ID: o. 53 (mm) I Soil Extract Volume : ____ (uL)
Lab Sample ID: 9809144-02
Lab File ID: 0914402
Date Sampled: 09/23/98
Date Analyzed: 10/01/98
Dilution Factor: 1.0
Soil Aliquot Volume:
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I
I
I
I
I
I
I
I
I
127-18-4--------Tetrachloroethene
108-88-3--------Toluene
71-55-6---------1,1,1-Trichloroethane
79-00-5---------1,1,2-Trichloroethane
79-01-6---------Trichloroethene
75-01-4---------Vinyl chloride
1330-20-7-------Xylene(total)
FORM I VOA
1. 0 u
1. 0 u
1. 0 u
1.0 u
1. 0 u
1.0 u
1.0 u
(uL)
D
I
g
g
FORM 1
PESTICIDE ORGANICS ANALYSIS DATA SHEET
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Lab Code: NA Batch No.: NA SAS No.: NA
Matrix: (soil/water) WATER
Sample wt/vol:
%-Moisture:
CLIENT SAMPLE NO.
W-20D
SDG No.: EPE.P9144-01
g Extraction:
1000 (g/mL) ML
decanted: (Y /N)
(SepF/Cont/Sonc/Soxh) SEPF
Lab Sample ID: 9809144-01
Lab File ID: 023F0101
Date Sampled: 09/23/98
Date Extracted: 09/29/98
Date Analyzed: 10/17/98
Dilution Factor: 1.0
Concentrated Extract Volume: 2 (mL) I Injection Volume: 0.S(uL)
I
I
I
I
I
I
I
I
I
I
I
I
GPC Cleanup: (Y /N) N pH: NA Sulfur Cleanup: (Y/N) N
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
309-00-2--------Aldrin 0.010 u
319-84-6--------alpha-BHC 0.010 u
5103-71-9-------alpha-Chlordane 0.010 u
319-85-7--------beta-BHC 0.010 u
72-54-8---------4,4'-DDD 0.020 u
72-55-9---------4,4'-DDE 0.020 u
50-29-3---------4,4'-DDT 0.020 u
60-57-1---------Dieldrin 0.020 u
319-86-8--------delta-BHC 0.0078 JBP
959-98-8--------Endosulfan I 0.010 u
33213-65-9------Endosulfan II 0.020 u
1031-07-8-------Endosulfan sulfate 0.020 u
72-20-8---------Endrin 0.020 u
7421-36-3-------Endrin aideFiyde 0.020 u
53494-70-5------Endrin ketone 0.020 u
58-89-9---------gamma-BHC (Lindane) 0.0048 JP
5103-74-2-------gamma-Chlordane 0.010 u
76-44-8---------Heptachlor 0.010 u
1024-57-3-------Heptachlor epoxide 0.0014 JP
72-43-5---------Methoxychlor 0.025 JBP
8001-35-2-------Toxaphene 1.0 u
12674-11-2------Aroclor-1016 0.20 u
11104-28-2------Aroclor-1221 0.40 u
1114-16-5-------Aroclor-1232 0.20 u
53469-21-9------Aroclor-1242 0.20 u
12672-29-6------Aroclor-1248 0.20 u
11097-69-1------Aroclor-1254 0.20 u
11096-82-5------Aroclor-1260 0.20 u
FORM I PEST
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
FORM 1 CLIENT SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
PBLK0l
Lab Name: ECKENFELDER INC. Contract: EL PASO ENERGY
Lab Code: NA Batch No. : NA SAS No.: NA SDG No.: EPE.P9144-01
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
decanted: (Y /N)
(SepF/Cont/Sonc/Soxh) SEPF
% Moisture:
Extraction:
Concentrated Extract Volume: 2 (mL)
Injection Volume: 0. 5 (uL)
Lab Sample ID: METHOD BLANK
Lab File ID: 021F0101
Date Sampled:
I Date Extracted: 09/29/98
Date Analyzed: 10/17/98
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: NA Sulfur Cleanup: (Y/N) N
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
309-00-2--------Aldrin 0.010 u
319-84-6--------alpha-BHC 0.010 u
5103-71-9-------alpha-Chlordane 0.010 u
319-85-7--------beta-BHC 0.010 u
72-54-8---------4,4'-DDD 0.020 u
72-55-9---------4,4'-DDE 0.020 u
50-29-3---------4,4'-DDT 0.020 u
60-57-1---------Dieldrin 0.020 u
319-86-8--------delta-BHC 0.0015 JP
959-98-8--------Endosulfan I 0.010 u
33213-65-9------Endosulfan II 0.020 u
1031-07-8-------Endosulfan suil'ate 0.020 u
72-20-8---------Endrin 0.020 u
7421-36-3-------Endrin aideFiyde 0.020 u
53494-70-5------Endrin ketone 0.020 u
58-89-9---------gamma-BHC (Lindanel 0.010 u
5103-74-2-------gamma-Chlordane 0.010 u
76-44-8---------Heptachlor 0.010 u
1024-57-3-------Heptachlor epoxide 0.010 u
72-43-5---------Methoxychlor 0.0079 JP
8001-35-2-------Toxaphene 1.0 u
12674-11-2------Aroclor-1016 0.20 u
11104-28-2------Aroclor-1221 0. 40 u
1114-16-5-------Aroclor-1232 0.20 u
53469-21-9------Aroclor-1242 0.20 u
12672-29-6------Aroclor-1248 0.20 u
11097-69-1------Aroclor-1254 0.20 u
11096-82-5------Aroclor-1260 0.20 u
FORM I PEST