Loading...
HomeMy WebLinkAboutNCD095458527_19910114_FCX Inc. (Statesville)_SERB C_Pre-NPL File 1986 - 1991-OCRl _.,1l \J sr,.,.,.,1, ...,,.,....._ :,.\J ' --7. 'S'>Ta ~ > < \ 4 ,. 0' "''◄t PA01~ LJN,TE~,i~ES ENVIRONMENT AL PR0T,~ION AGENCY REGION IV January 14, 1991 . Ms. Pat DeRosa, Heao CERClA Branch Superfund Section ENVIRONMENTAL SERVICES DIVISION ATHENS. GEORGIA 30613 Division of Solid.Waste Management P.O. Box 27687 Raleigh, North Carolina 27611-7687 Dear Ms. DeRosa: ffiftl'i::111ED J,41v 1 B SUA 1997 'EHFtJrvlJ S£crto111 I just wanted to take a moment to thank you for sending the copy of the Site Inspection Report forifCX:Statesvil·le{ The prompt turn-around was especially appreciated. Among the referenced materials attached to the report were several documents that I had been trying unsuccessfully to track down. Once again, your assistance is very much appreciated. for you, please do not hesitate to call. Thanks. S~y~ Don Hunter, Hydrogeologist Superfund Unlt Ha'7~....-.-1r'11C' T,Ta<"!t-O C::ar-t-i nn If I can ever do anything " ~ '-1 r;. t , ~~;;;;;;.--·~~'· '·o ,.,,,.,,~,, ~ .ja,., 1 .'.'/~,I .~~ ~;6J~.rf;j I . ., .,,,,,,.,,, ' 1· ~Q,, • .,,;<> State of North Carolina -t Department of Environment, Health, and Natural Resources Division of Solid Waste Man~gement P.O. Box 27687 · Raleigh, North Caroli~a 27611-7687 I James G. Martin, Governor William W. Cobey, Jr., Secretary Mr. Don Hunter 4 January 1991 US EPA -Environmental Services Division College Station Road Athens, GA 30613-7799 Subject: FCX -Statesville, NC NCD 095 458 527 I I D.ear Mr. Hunter: I William L. Meyer Director E~~losed please find a copy of the Site Inspection Retort for the FCX -Statesville site as per your telephone request of 3 January 1991. j If you have any questions, please contact me at (919) 1733-2801. enclosure · PD/kc/pat. 020 Sincerely, I Jilt-~ . I Pat DeRosa, Head ' . CERCLA Branch Superfund 'section I I ...__ e ii { j i I. II I L ~ t: -: ~ a I d J~ ~ q) ~~ =ef j.. ~ '1 ,,-../ 0 vi ,1 -1 --0 ~ I ./ J J <J j; ~ () ,r ~ _J., _,, cli Q ' . ii ii) ~ L.. I ~ __., '' ~ 'j_ ,i '0-, l d 1 I-I/ ,\' 1--c{) 0 j... l--1 ·i: Jo::? q ct) ca c,t;/. c£.J (? -1 "'1 1: (. r6 J·-~ , j f• / ../ ~ co 1 r-1 60 ,->f d 6~ ,. 1/,1 ~'7 ~ .· re v L-' v:J~ .d~ ~<II <j \,.\-. 0 @ e €l ~ L Cl j .•·· .i. • • IN THE ~ STATES BANKRUPTCY CXXJRr FDR THE *•N DISTRICT OF NORTH CAROLINA. ! Case No. S-85-01574-5 ATTACHMENT 4 Il! RE: FCX, Inc., ) ) )_ ) Il! PROCEEDil!GS FDR THE REORGANIZATION OF A CDRJ-ORATION D2btor ) ) CHAP:rER 11 CASE NUMBER S-85-01574-5 AFFIDAvrr OF iliis B. WALKER, DATA MANAGEMENT ·o::oRDINATOR, SUPER.FUND ERANGl, SOLID WASTE MANAGEMENT SECTION, DIVISION OF HEALTH SERVICES ,I DEPARIMEITT OF HUMAN RESCURCES, STATE OF NORI'H CAROLINA. I I I I.Dis B. Walker, be:i.n,/ first duly sworn, says; ' . 1) that khe is the Data Management Coordinator of the North carolina Superfund Branch, an agency of the state of; .. North caro~ina, in the office located at 401 Oberlin Road in Raleigh, Ncirth carolina, and is duly authorized by the North carolina sJi::=-furd Branch Head to TIBke this affidavit on its 001alf; I 2) that ,from and after 1 July 1985, she was the Data Management I Coordinator of the North caroljna CERCLA Unit which later became the North carolina Superfund Branch and, as the Data Management Coordinator and custodian of -1 • • • these records, has provided an analysis S1.l!llITl3rY of the Cost Recovery I records of that Branch =ncern:i.n;r the investigations =iipleted by the Branch staff at the former FCX facility in Statesville, North carolina and at the former FCXifacility in Washington, North carolina; and i 3) that the attached Cost Recovery forms from and after 17 Octobe:rj 1988, expense a=unts, travel legs, telephone logs, invoices and bills are true and =rrect =pies of the originals; -i . . all statedj this the J f-Cf day of January, 1989. ) I ub ibedt l. s scr ai sworn to before me -' this the ,jf'; .day of January, 1989 . i}f .. ~ A xQ ) ./1..J.--&<'..,O-...,, ~-'C) {)(,,j, _Q,,,v.___ . otary Public I _ My Commission l';XPires I d -Io-<? °t I • • • I. II I I I I I _ j . .,, ' I I • • CDST RECOVERY ANALYSIS SUMMARY FCX -STATESVILIE NCD095458527 Oci:ober 17, 1988 -CeceiTiber 3i, 1989 1 .I f'ts ( Personne & Fnnge Bene 1 1210, 1810/20/30, 8312) ' i Total ATTACHMENT 4 , • -Staff Member Date ·.I Hours Incu=ed Total Salary Fringe Benefits Cost 20%/Personnel S. Atwcxxl C. Varlashkin S. Atwcxxl I 10/17/88 45 10/27/88 18 11/1/881 1 II . Travel (3111) , $ 638.10 223.92 14.18 10/24/88 Mileag~ -·365 miles at i .24 = III. Supplies (2390, : 2600) I I 4 tyveks@ $2.76 = $11.04 2 pr. nitrile gloves@ $1.75 = $3.50 2 pr. cotton gloves@ $.75 = $1.50 rv. Other (3990) I I 127. 62 44.78 2.84 I.ab Samples 10/25 -6 organics@ $194.00 I STATE BUI:GEJ' CDDE 1830-8312 ., i 100% State Funded Expel1ditures . ·I I $ 765.72 268.70 17.02 1·,051.44 87.60 16.04 1,164.00 $2,319.08 • • • I ,\• I i I ·I I ! I i ! I I COST RECDVERY ANALYSIS SUMMARY FCX -STATESVILIB NCIXl9.5458527 October 17, 1988 -Januar:y 1, 1989 I. Personnel & Fringe Benefits (1210, Staff Member Date I Hours . Salary 1810/20/30, 8312) In=ed Per Year Salary Total. Fringe Per Hour Salary Benefits I 20%/Personnel S. Atwcxxl 10/17 /BIB c. Varlashkin 10/27 /818 S. Atwcxxl 11/1/BB! I I II. Travel (3111) I 45 $29,508 14.lB 18 25,884 12.44 1 29,508 14.18 10/24/88 Mileag~ -365 miles at .24 = III. IV. I Supplies (2390, 1 2600) I 4 tyveks@ $2.76 = $11.04 2 pr. nitrile gloves@ $1.75 = $3.50 I . 2 pr. cotton gloves@ $.75 = $1.50 I Other (3990) I Lab Samples 10/25 -6 organics@ $194.00 I ! ,I i I i I I i I I I I I 638.10 127.62 $ 223.92 44.78 14.18 2.84 'Total Cost 765.72 268.70 17 .02 ------- 1,051.44 87.60 16.04 1,164.00 $2,319.08 • • ,I ' SITE NAME fC)< ·STATE ID . r REDJVERY DXDMENrA'.l'ICl'I y· csumrr '[O I:M:) . I STATE SITES . 5±-:3+e :SIi: lie-EMPLOYEE NAME s+,),') A-I-woe> J POSITION Tox;calo(J is T EPA ID PROJECT IEADER S±sn A±<c?~• d I INVESTIGATION Di'.'I'E.S :I CCOJMENTATION FOR') I EXPENSES IllCURRED! i I 9g g- ( 2EAR) Transportati,;m (In-State, Out-state) I Subsistence (In-state, Out-state) i SUpplies (Film, Maps, Ice, Etc., attach receipts) I· Health & Safety Equipment (List#) I Laboratory Samples I Soil: Water: Other: ' __ org. org. --org. $ ____ _ $ ____ _ $ ___ _ __ inorg. __ morg. __ inorg. ACTIVITY I DATE(S) 1. B3.ckground siparch, Evaluate Data 2. Prel:iJninary ~azard Ranking Score Assigned ' 3 . 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. Hazard Ranl<:ihg Score Finalized & Site Placed on Priority List I Prepare Study/Safety Plan Conduct Fiel~ Work: Field T:iJne I Travel T:iJne Sample Preparation/Lab Delivery I Review Analytical Data . . . ~ Envirorrrnental Impact Statement ' Written Declaration I Consent/Compliance Orders Public PartiSipation Plan Evaluating &I Approving Remedial Plan CoordinatinglRemedial Action Plan i ' 11/1 ' Total , -~ru?eor~ I I . DATE FOSTED _L~-;'30c=..,·_'c_~----- (Attach Daily Bre),kdown and Telephone List) ._, · .. - ·<~~-:.,;.:~,-•. ,....:, . Tof,i]-Miles ·· I e--'-TRc,l.:.P_,D:;cA:,:TccE=.S -+-c_ ___ ·=-0,_,FF_,_1 C::.1'.'.:A;,L_T:.cR'.'.:A,_,v_,_EccL· ___ ~-IL--~--'-----'D~R_,_1.:.v=-ER.:.'s:'..,,;: .,cc;,0i'.c·r_,_1 F_,_IC:;A:cT:.cl=.Oc:N_.:__1__--4··. ·_.: ?iX· ODOMETER leave Return From ! To Purpose of·-.Trip .,,_, · . Signature.· ·._., READING· MILES . TRAVEU: ,. ? .. t)~l_.,/4 ~ :~./., :-."/ :./)h' <~l'ij,' ~ ··1.,..,()-<_. . I . . i~_/:>.£~- I . ,' ' I -0 V ' IN • t--c--t~.-,'-c•+l---,-~---.:__+--".1,-----c----+--'----'-=~~---'-,----'-,l--'----'----"---c-'--:-'.~,-::.•-. ---l-~:-;-:-1-1,_·,t.29,i_J:___.-1-:__~ '"· f--,---+----'+--__:___,_~+1__-,---:-----+-'--'--___.::___.::l___---Ji__l__l_____.::~_c_i-:::::.'._j_1_____.::___.::j_~ IN I, ·OUT : ., • • I I ·1 • rosT ~SlJEWT~~CNrr S.I'ATE Sr:I.'ES SITE NAME FC-'f-fShtes0:)le... EMPLOYEE NAME StAo A±woad. STATE ID s, s LJ 90 roDGol .3 rosmoN Tv y.; Lo\ 05 is: t-- ·1 "' EPA ID IJL-b095':/:SG52 7 PROJECT LEADER S+!lo Ah,20Dd I INVESTIGATION DATES I I DXUMENTATION FOR: ,1 •I I O 'J. Octo'be., (MONTH) /9~8' (YEAR) EXPENSES INCURRED: TranspOrtat~on (In-stat§, out-state) $ 8 7./,,,0 (3l S,.je.J d 0.2.4 SUbsistencej (In-State, out-State) $ ____ _ Supplies (Film, Maps, Ice, Etc., attach receipts) $ Heal th & sakety Equipment (List#) Lj ±:i v.c.\::-' 2 r C D :\.-r ;-\e.._s_\._u<_$_2_f r ( 0 tt"" q 1 o, I @ 5-:-t° O I @, ') o o 'J 1 © ~ laboratory Samples Soil: -~o_rg. · __ inorg. I ' Water: G org.k __ :jnorg. Other:, __ org. __ ll1org. bCTIVI'I'Y DATE(S} HOURS 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. Background Search, Evaluate Data I PreliminaryjHazard Ranking Score Assigned I Hazard :RanJs..:j..ng score Finalized & Site PlacedJon Priority List Prepare Study/Safety Plan I Conduct Field Work: Field Time j Travel Time Sample Preparation/lab Celivery ' Anal),+. Review x~ical Data . . . . J Environmental Impact statement . . I Written eeciaration I . Consent/Compliance Orders ' 11. Public Participation Plan I 12. Evaluating & Approving Remedial Plan 13. Coordinat~ Remedial Action Plan !lo 10/2) s /Vl2-~ s I 0)2.oJ G !oh-~ 2 I /o/272i3J· I ) 13 I -=Total Lt s : . igna :: -4.k?oiilr DATE rosTED p~u.O 0 ~-C P... to ~,;,__-e· I' 3 ! J? r (Attad1 Daily Breakdown and Telephone Llst) ~ / ¼/ * S,t-~\e..\ -1--l 0 Mor-;\or:~ w~\ls · 2fl.... -\:,,1\ e../.,..e...v..1't-~l ; e... re.r, -\-; c: l '2.-:1 ' '_ \ • • • ! I .FC>'-S-\-/t re-sv; \ \-e . / Los-\-l2-eco0c.r)' Sv..""""~ . I Oc..:\-0 ~e., l'°i'i?c "01'\:l7 ?,eA-f=.J I -{].o, 5-i-l'r" . A f-v-Joo d._ . Oe11 'i ·I A C ± ; V; +-/ ! .B1tc½,o"'~ d. .)~rc..h / ev,.,(<-<..,,..+e I , BAc..k_yo"'~d se.14,.J.-. 1 e i11t-!"'rFI-"'-- , Pr<'.fA•e..-S;t,c,! s+-d1 p )11n i;C.ond0c...+ t-,':-:..\d. worK • s"""'f\e.. f re.r~rA-t; i) Y1 •• f2_e.v;ew Af\A-tlt:'-A) d/1--/-f/ . l •• _{2,e.v:e_w ,4 nA-ljti'cA l cl.A.-+fr ,' /Ze,v;ew A "A.11/ih",t-/ d,.,1-A I ' "I I i ·I JL~- 1 . I I I i ' . I I I I ,\ I 1),4\-~ df)-+P, Ju/1 7 drt-f-A ID/ tr 10/21 10/2..; / D /2 5 /o/ 2 7 Jo/2-c;; 10/_11 Toh+/ Hou.r .S: f- Ii- 5· '71 2 2 5 ~ L/5 • • .j • CDST RECOVERY D:X'UMEITTATICN aif,EI' (SUEfilT '.ID a«:) .., I STA_TE SITES . SITE NAME _F_c___y._~·._s~t~0~+e.=S~J_:~lle..-~_ EMPLOYEE NAME c.~,,,. ..... )o\:t-e.... \JAr\1>rs\t,;/\ I STATE ID .>\Sc\'7010061?, FDSITION J±yd.-rDjeo\o;ii.sT EPA ID ;V C. J)O 9 S l/ S 8' 5 2-7 PROJECT LEADER S +-A-"' A:\:0oad ' INVESTIGATION DP.TES I i CXXUMENTATION FDR: ., ' i EXPENSES INOJRRED: 0 'J.. D c\--vl,~ r (ffiN'l'H) IC/ 'c'?" (2EAR) Transportation (In-State, out-state) I Subsistence1 (In-State, out-State) I Supplies (Film, Maps, Ice, Etc., attach receipts) I . $ ____ _ $ ____ _ $ ____ _ Health & Safety Equipment (List#) ______ · ______ _ I . Laboratory ~amples I Soil: Water: Other:. __ org. __ org. __ org. __ :j_norg. __ :inorg. __ D1org. ACTIVITY DATE(S) HOURS 1. 2 . 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. Eackground Search, Evaluate Data Preliminary-I Hazard Ranking S=re Assigned ' Hazard RanJ¢.ng s=re Finalized & Site· Placedlon Priority List ' Prepare stufy/Safety Plan/Tr;p Re.rorf Conduct Field Work: Field Time \ Travel Time Sample Preparation/Lab Celivery I Review Analytical Data . I Environmental Impact Statement I . Written Ceclaration ' Consent/Comi:iliance Orders 'I Public Participation Plan I I Evaluating & Approving Remedial Plan ? 10/21,25,20 10/14 1072 4 • Jo/z5, ' Io /11 ' h 3 G· 2. 13. Coordinating Remedial Action Plan I Tota1 t 8 . I r~t~. I .1.cjnaeot ~ DATE FOSTED_ p~,4J S-&h .-c ;2., -z:i-d.£.~ 1,, /J ; t-r (Attach Daily Breakdown and Telephone List) 6;z:,/ ~ / ?t..u . I ' I I • • : I i. • Fcy. -s+.,.,,-tesu."/1-e I 1°st T2.<2-c.00ery Su..""'""'-t-rj ib (_ +-D I., e_ ' I c; f;' S- I . -,. t0 , C~r1-r\o\1-e__ Vt1,l-tshk;n I . I I : . T..-; (' f ref A rA t; Of"\ / s A -te.. +7 p / q n : F; c.. IJ w o t I<- , . + I t lJr;fe__ r;fl fC..fb• ·. SA""-fle_ preel ... IA\, de\;~ .. i,J,;+e. +,...; f, rE'for+ ?;cl"'-'-f tJ-rev:k<-,J / .4-'b d,1-j-0 I ' I I I ! ! i i I I I. I I I I I ID /2 I · JD/2.. cj. . 10/2 S )0)25 } 0/2-& )9)2._7 j 3 9 2 2. I ' PURCHAS1NG REQUISITION . . ' ie TO: Department of Human Resources -Purchasing FROM: Division of Health Services!-4430-0000 NORTH CAROLINA DEPARTMENT OF HUMAN RESOURCES · DIVISION OF HEAL TH SERVICES Requisition No. _________ _ 11-16 19 88 .OJECT: Super fund DATE ' ---· PLEASE CONTACT: I Patricia SUBHEAD: FUND __ l=.8::..:3::..:0'-----'-I FUNDc..· ____ _ I Bowden OBJECT __ 2_3_90 __ OBJECT ____ _ · q19-733-2801 . Phone No. __ . ___ _ 8307 RCC _____ _ PROG __ 2_08_6 __ _ Code 14 RCC _____ _ PROG ____ _ Code I 'i .., . ...:c:·S:.::Bc::.:l:.::.P:c:.T::.:O=-c..: --'D::::.:_IV:._l:.::Sc:.IO::::.:_NccO::::.:_F.:c.I1c::.:E::..:·A..:;L:::-T:::H:.:..::S:.::E:.::.R:.:Vccl:.::C:.::E:::::S'---- Solid waste Management Section _._ ... '_/o ____ ~s~uperfund Branch1 CHARGE TO: DIVISION OF HEALTH SERVICJ 1 401. Oberlin Rd./PO Box 2091 . ' Raleigh, Ne 27602 ATTENTION: Budget Office Division of Health Services P. 0. Box 2091 Raleigh, North Carolina 27602-2091 QUANTITY CAT. OR PART NO. I ITEM. DESCRI\'TION UNIT PRICE TOTAL PR! (on, -p· 8'7.5--9i•IL ' 30pai LA2057 ILow ·cost latex boots size XL 6.S0pai· 195.00 (Li/YI .p L/ 7 S-1( D ; ..... 2 doz LA5677 IFlock Lined Nitrile Gloves size 10 21.10 de 42.20 " (!.0/71 ti "I 75'-4/0 ' l,1<, ' Nitrile Gloves size 8 21.10 1 doz LA5677 JFlock Lined Ya f< e;om.-n JJ. ;uo 1L1 .. 'EO 21.95 65.85• 3 LA-:1453-2 IEye wash station I (]u/'rl-/1 J,o,5 .. J'7.-().f( !Pocket guides-NIOSH Pocket guide to Chemica Haz. 10. ,o 60.00 6 . LA-2011 I bags-yellow-36x63 -55 gallon 73.25 carton/5 per carton ii ES '29 6 mil I : I I I Lab Safety Supply I PO Box 1368 I ' Janesville, 53547-1368 I WI I l-800-356-0783 Federal IDl!36-2685918 EX PLAN ATlON: Required for major cquiplcnt ice ms and items of unusual nature. This rcqucst (represents an 457 _,, initial purchase} (is requcs{ed to replace similar eQuipment which has been or will be disposed of, worn out, etc.) lt will SUBTOTAL be used (or (brief explanation). Attach exrra sheC1s if necessary: I SALES TAX 22.l : Jjf}{). ,: i Ap fov/, b: GRAND TOTAL I I .Fund, for thi6 purpose Uc :l.\·ail:i.blc. I Scccion Chic( Budget Officer Dace Supporcive Services Administrator Controller (If !oca! i.s $2500 or more) D, .S~IP TO: ' le .I. I DIVISION OF HEALTH SERVICES Solid and Hazardous Waste Mgmt.-Br. Env i ran men ta 1 H e..altb~l~s,.,e~c~t~i"o"-n"-·------- ' PO Box 2091 . -. ·._: .-· r.~1 ,7-•·-~-~-'.-':";:~-'.~.f·}M~ CHARGE TO: DIVISION OF HEALTH SERVICES··· . ATTENTION: Budget Office '---------"'Ruleigh, NC 27602-~2-'<!0,;.9.,.,l-------' Division of Health Services P. 0. Box 2091 .. 1 Bath Building Room 203 , • I Raleigh, North Carolina 27602 1:-,.·sTRJJCTIONS: Detnile<l specifications', when' applicable, to be submitted on nn atlachcd·aheet. Show manufacturer's name and catr~ I,..~ I . r.::mb;er. ··When ordering repair parts. give 1 make, Jnodel and serial na mber of equipment for which parts arc needed. QUANTITY CA.T. OR PART NO. 117100 1=moR CONTACT '"'D .. TD JI ITEM -DESCRIPTION UNIT PRICE I Brown Jersey, Clute Pattern, Knit Wrist Cotton .75 ea Gloves. COMM// 200-27. MAN'S SIZE LARGE. pair I I ;I l 5% '1IX 'T'()'T', Katrina Smith 872-1120 51, 0892716 EARLY DISTRIBUTING COMPANY 2816 Brewton Ralei<>h. NC PL. 27604 ' ; i S 18. 00 .90 1Q qo___ EXPLANATION: Requii-ed for major eQuipment items .and items of unU!-ual nature. This request (represents an initial purchase) (i! c;·uested to ·replace similar equipment .l.tlach extra ahcct.s if necessary: :·unds for this purpose nre a\·ailnblc. 0lJOCET OF'FJCE;:i: ' . . which has been or wjll be dii,pos ed of, won, out. etc.) It will be used for (brief explanation). ! .i I I I i I I OATE Approved by: __zj-_/',V-,-. ,I; ::;.~_R_Lr_.L__ URANCH HEA.0 / / SECTION CHiEF SUPPORTIVE SE:RVtCC:'.S A0MlN1STRATOR COt-:TROLLER Dntc: /u Ir I.;, I I ,,::"tJJ.jJJ,@,~~<,,)~ • •:·'''.•?c'" ··.·~•"' c""T'' •• .. •· · ' ' " · • · C10.s!l i (ic,; tio"; Project __ ,cC_,,E,,,Ro,CecLA=~-------Subhead __ _c'l~8~3~0-:.=~2~3~9~0~--8=3~0~7_-~2~0=8~6c_ ____ _ Code '.!.;02i SHIP TO: DIVISION OF HEALTH! SERVICES CHARGE TO: DIVISION OF. H8ALTH SERVICES Solid and Hazardous ,Waste Hgmt. Branch Environmental ·Health: Section Rm: 203 i 2D91 ATTENTION: Budget Office Division of Health Services P. 0. Box 2091 PO Box 2091 Raleigh, NC 2~602 .Contact: Patricia Bbwden I 733-2801 Raleigh, North Carolina 27602 INSTRUCTIONS: Detailed specifications,· ~hen applicable, t.o be submitted on an .attached shceL Show manufncturer'5 name and catalog ' number. When ordering repair part.a. gi\'e ffiake, model o.nd serial nu mba of equipment for which parts are needed. " •. . . . .. I .. ~.-.. QUANTITY CAT. OR PART NO. ! ITEM • DESCRIPTION UNIT PRICE TOTAL PR/CE I Regula~ d-lq-<iJ ca·se-(25/, ase) II 1015 MEDI~~ 69.00 :).38.00 :· ,. 2..; 0 -~ COHH .. I /1 34 8-1--S-~ ' -. ;)-0-A.½ -) , _, ----·· case ( 25/ I ase) 1/4015 Medin:'l)l size Saranex Coated Tyvek 221. 33 221. 33 I Comm. I II 345 08 15 ~··'--:ir-n -:)') I .. I c.z-t-·· 1 7 96 I I m -t,a..l 0077 00 • . I ,[ VENDOR: Jonei Safetv Supply PO Bcix 4190 I Greensboro. NC 27403 VENDOR CONT. :,CT: ¥ndy:Honger FED. ID I/ 540 73 7369 ! I Contact: P atrici~ Bowden DHS 733-2801 I ' I I I ., ... EXPLANATION: Required. for major equipment items and items of unusual nature. This request (represents an 1n1tial purchase) (1s re- quested to replace similar equipment which h1na been or will be dispos cd of, worn out, etc.) It ~di! be use<l for (brief expl,rnation). I Attach extra sheels if ne-cessary: Funds for thi:i purpo:;~ nrc n1·ai\n\Jle. OHS F'orrn ll:i~tl{,,1·. llJ-.:::::1 Budg-cl Offi,;c• OArE: Appr'ovcd by: /() /c, I i:'...Z I I su,Poen1-.,e: SF.RVICC5 /\01-11;-..';5':"RATO~ • es, • I I • • I I CDST REffiVERY ANALYSIS SUMMARY I FCX -STW'ESVIIJ.E I NCD095458527 I I I. Personnel & Fringe\Benefits Staff D3.te Posted I Type of Salary, Salaryjhr. Total NO.* Hours iEvent Hours Year Cost 40 6/86. SI 12 29,988 40 9/86 SI 2 31,260 21 3/86 I PA 29 27,204 21 6/86 'SI 75 27,204 21 9/86 I SI 47 29,460 I 37 6/86 I SI 22 24,792 37 6/86 I SI 13.5 24,792 37 ·6/87 1 sI 19 25,992 37 6/87 ·1 SI 17 25,992 37 9/87 SI 2 27,288 ' 37 12/87 f SI 1 27,288 37 3/88 I or 1 27,288 ' I i II. Travel (3111, 3112, \3121, 3122, 2500) 5/5-87 Mileage & 283 miles at 22.5 5/6-87 In-state ~istence (No. 21&37) I 65.93 102.00 i III. Equipment (5100, 5200, 5300) I IV. Supplies (2390, 2600) . . I V. -I Staff. No. 37 4/10 f SI 12.50 37 4/13 j SI 2.00 37 4/20, SI 1.00 21 5/06 \ SI 2.97 Contractual (6929) I I I I I -i I for maps for copies for copies for ice 14.42 15.03 13.08 13.08 14.16 11.92 11.92 12.50 12.50 13.12 13.12 13.12 Cost 173.04 30.06 379.32 981. 00 665.52 262.24 160.92 237.50 212.50 26.24 13.12 13.12 3,154.58 167.93 18.47 • FCX-Statesville Cost Recovery Analysis Sumnrn:y Page 2 _ 1 ·I VI Other I 3990 Lab Samples: 5/7/86 I 5 VOA 114 Organic : 14 Inorganic ·1 @ 194.00 $ 970 @ 194. 00 ' 2716 @ 100.00 1400 5,086.00 I ._ · -vr:t' Indirect Cost I 30% of 3,103.34 = 931.00 15.1% of 51.24 = 7.74 • • Indirect cost to.June 30, 1987 was 30% after 15.1%. KEY TO STAFF NUMBERS* 21 37 38 40 KEY TO TYPE** I I Harry Holladay I Grover Nicholson Pat CeRosa ' ' i Mary Giguere PA Preliminary Assessment SI :site Investigation 938.74 $9,365.72 CJI' I Any activity other than Preliminary Assessment .\ or Site Investigation I ' Prepared by:. Lois Walker 10/13/88 1005 I ' Data Management Coordinator I I i I ' I i ' Ji~-il{~:¢=j~~-~}~~~~u•·;·---2~-~.~~:~::££2lE2~_-· ~~~~ .. ~-;~.1 JN~TRllc-tiONS;·:· · ·· .·. ! • · sTAi-i::: OF NORTH CAR0L1NA •. 1. .-_s~~e 1_0· e~ch driver of perm,rnenrly I .. , assigned vehicle. PARTMENT OF ADMINISTRATI ' ~ 2. Driver makes entries for each trip. ; MOTOR FLEET MAN AG EM ENT DIVISION /.. ?3. Al end of each month: send white and I ~ RALEIGH yellow copies lo agency budget officer,· ., ._s'/ Rafe per Mile 1 . I Mileage I Charge I Miflimum Amount pink copy stays in vehicle. 01 __, / / / / /t:J ~ 4 .•. ncy budget officer sends while ·I ~ TRAVEL LOG //Cf '(D 10 Motor Fleet Management. f-----, ------1 5. Motor Fleet Mana9emenl bills agency. •FOR PERMAN£'.NTLY ASSIGNED VEHICLES To1dl Amount 1 Ap~roval of Agency Head or Supervisor: OFFICIAL TRAVELI DRIVER'S CERTIFICATION I To Purpose of Trip Signature J/ fl . ·. I ruc,e.. Pi'ne /1oJe.,t h Number of Trio Davs ' Local TripJ ' Odometer· Reading 1: Dept./Off. No. Fund No. RCC No. . ·-·-· ~ ODOMETER READING Fo, /r'ic:.11. f 19/3_ MILES TRAVELED 100 /75' 4o • • • i I I · North Carolina Dep;irtrnent of f-Iuman Resources t . . • . 325 North S,lisbury S<reer • R,lcigh, Nonh Carolin, 27611 . . 1 . James G. Manin, Governor I · • · . David T. Flahcny,·Secrcmy MEMORANDUM I I I I I I I November 24, TO:_ Division! Directors FROM: Allen Garill !l/::,1,cW RE: New Budget Manual 19 87 I . Each of you should have received a new Budget Manual·that became effectiv~ November 1, 1987. Attached ,is a copy of the trans~ittal letter from Marvin Dorman that should have been attached to each manual. Mr.· Dorman's·memorandum highlights major -cliariges in the new mariual . . · . . . I . . . the )lease not,e .that the IRS rate; for those employees requ~stin~ ieimbursement at that rate.when the IRS rate is lower than the statutbry rate per mile, has increased to 22.5 cents per mile. · The new iIRS rate became effective January 1·, 1987. · .. Division Directbrs have the discretion of allowing employees to file,_ ameri'ded reimbursement requests to recoup the difference between the 61d'1 rate and riew rate effective July 1, . 19 8 7. Prior year fund~ a're .hot available for the period Janriary 1 ~ June 30, ... 1987 .. Also not~ that the 25 cents/mile reimbursement for use of· ,.· ,·, . 'I . . . . •. . personal 'vehicles has decreased from 75 miles· round trip to 60 ·miles/round. trip mileage. · · · · · ! Should youi have contact your Program ALG/JQS/llr I I i i '! I i questions regarding the Analyst in this _office. ne~ manual, ple~se ' !. 0 I ~! ~ s/f" -s-/1-/ cf'G • i ;-/&-1 ~ l /3/J e u~ 1 /I/ <2 V;e c;_,---c¾ ~6--CU) .. o10/ct$\ I ., -.. /:?--ct_J! ~ ~-L~ . / y 3 /X-(./4 / Uf7 . . . •.··· ·. .. . i -.. . . . • 2. , ... Ft!Y ~c.'~ //tic__ . s /-;z./£$ I . 1·· ._. -... I t. ,. I cSL--~r ~f/-0 Vd c ~ /'t>U~f,,r ?i°-Y--/2 o-/1-, ······/L-% • :rJ6 -JY3l·=. c2Y3 ~ I 1 I ., I i I ' .......... ·····-············ -r·· ·····-·· .. -····--·····----··---.... ·-· . --... I . I a-o r.1 l:, ~ :4 . FC!.__,k:-·. ; . ' . . -,· ' ....... ----···--· .. . -· ···-·----------· ... -.. ___ ,.,, , __ ·-.... -., ....... -·---···---···· 0 I •I I . . . . . . I . I 1 ·· .. . I I .1 I I ' 1-JORlH L-Al<VL\'"' 0f'.HIJMAN 8ES()URCES :?{HEALTH SERV,ICE. 'REQUEST FOR ! Date '-0 ;__;:,_;~ JNL-40 D/0-4430 - REF# · lilt) i ID# 0 L 2.. ~.3_ 2 ~Q_ I Batch #40-_ · Fund Control Amount Cr Obj. RCC Prog ID .·.-:. s'Cii?SEMENT OF TRAVEL _;;-er AND I >···" I lEXPENSES INCURRE~ IN THE scHARGE OF OFFICIAL [?UlY- Y'.:'iNCLUDING PER DIEf.;1 ;~•.: . att'Privole Car@ .25/mlle Jn1o1e Prfvole Car@ .25/mlle .,_I_·----,--➔ ··o;,~-:. - . • -. I . . . J'n·'DHS Employee-Prfvote Car@ .25/mlle _____ ,, J 1i'v1 7500 7500 -" 7500 7500 7500 7500 7500 ·- -7500 I 3111 I I ½ 0 3112 i~ol 'JORI 11! • I 3121 I ( I 3122 -I - I I 3111 2 I ! i 3121 2 J I 2 · .. j: -I' ,~lt2:·· , I ( ··,-··, Tota\ Reimbursed s / 10 Audited by G/jTtON5 TO CLAIMANT: Prepa1ie original and (1) cop ;iftt:a,~9..submit the original to your 1 Budget or Business_ y. Staple all necessary receipts and other supporting documents to_ Office. Retain (1) copy. . - :~ ,.;;,.•··~ . . . . ·I I I I I Section/Branch -;;,' /-I W f" /JV IR. 0 ,J · Title Headquaners {City) , · ., aco (o 1s-f u. (,:, r,.______ _-1-,_=:::-=-=..:::.;,..f._!'!_.f___ ____ +-__,_;;;_::::..:._:'--'-)'-?~-- O ate ·---~ S-Jo -!:!~ -"--l--□-,-,e:::::__O_u-', ."o:::l .,.S_ia..:, e:c:::--,--,,D-,-, ec-o-:l-:E:--x-ce-,-,---1 less Adv a nee 5/, {10 Travel Auth. Allowance Auth. s-.110 -"dh Reimbursement Un pen2!ti~s of perjury I certify this is a tr'lie and accurate state· Jllent of the city of lodgirig, expenses and al\o~ances incurred in the I have examined this reimbursement request and certify that it is just·. .ind reasonable. services o: e S1a1e. __,J &,,_J . (CLA~NT) ! I ~~, (if~' (SUPERVISOR) Tr ave! (show each city visited) . Tramponalion Subsistence Other Expenses I Day! from lO 1'• ln-S1ate Out-of-State l' In-State Out-of-State Explanat.ion Amount s-~I ;2,..f<-->-1 51.1-,$,,,11.,, k 8 ■ /J,o<-<,_/e/ ? /1,1-r · ,;L, .,,/ A L .4-,oo 71,,,· /J. j /.Zco-P /Mr-f 0 D ?-,?"i Daily Privote Car Mileage: @ c/rnile p H -3;2.00 Total 43 ~.--iE <L.P-,,J;//4 /!,,_(.,_:;_, I. R 8 '<,7S' .J2.0iu=,{___£, P/n A L 4,0" 0 D D2.ily Private Car Mileage: @ c/mile p , H -Total q.,;:i.;- .R 8 ' r';l \. 'A L 0 D [-Daily PrivJ!e Car MilcJge: @ c/mile ,;p H I ••·• ill Tota! ;."~' ''"''' '(2)Typc of I Total Total }otal Total Tota\ ?. •I Cu Sub~i\lence In-Staie Ou1-ol-S!Jic T(ampor(, Transpon. Auth. Subsist. Auth. Subsisl. Other Exp. A-Brcald.nt S 3.25 S 4.25 I O-Oth1:1, r.1il 0: bu~ lunch 4.00 S.00 r-P1.-owned cu Dinner 7 .75 10.75 SI, (JD Room 27 .00 )4.00 foun eo-""°l 24-hr. period 42.00 54.00 I D~~ :',~ 1R~vi1~C 1/8SJ .:.i .. ' Employee's N2.me ··- LOCATION OF . .. . .. •. ·-· .. ·.•. I I ,•. . 0 f,c:,J-cs: </-;; //4 ,,UC-, • . . .. I " ' I ·I I DJVIS1.~)N OF HEALrti SERVICES i R-~~~ FOR OVERNIGHT TRAVEL ' i I ! I I Sec tion/Bran7c.h ' ' OVERNIGHT STAY (CITY) bJ?PROVED I . . 11 • . ' I I ~: I 0 l -,11 ' J!,,c-/ I k,~~ ~\J ·i P, .,;9 /,u;.,1 . u a v' i . ' ,· .. i I I I I ... . I . ' : i I ·, I i I ! ' ' I ' ' I I :, ' ., I I " I -I ' ' . I ; . I , I Month DATE OF 'BY APPROVAL &L'll i b • . ' • • rote Private Car@ .25/mlle . i ut-ol-Slole Prtvole Car@ .25/mll\' I X'i/ J / .JVU I II 1· I , / 1· d,..)! V IJ ,,.., . ll '"· ....... . •,•., 7500 I 3111 2 : 7500 I 3121 2 ' • i Non OHS Employee-Privole Car@ .. 25/mlle -----'i I I I /ZtJ 7500 I l/ Slc ()'\ 'r:,,19c '{;J]; BOY& 2 Total Reimbursed ' 9 /10 3 f') Audited by I 5TRUCTIONS TO CLAIMANT: Pre1pare original and (1) copy. Staple all necessary receipts and other supporting documents t( his form and submit the original to yciur Budget or Business Ollice. Retain (1) copy. . / /r:.-;,· ··. '.·' .... :_}/ q/;_f,__Ilf.. SER /JfcES '11) Divi~itin or Institution Section/Branch /--/ fill g_,_y _,_?-'-. _,_ll.co~u. tl D6 Y I Soc. Sec!# Payee's Name ~-- Payee's Addresi From (i 1 .. Period covered by this vollcher I }J;:, I To Title Date Date Out-a( State Travel Auih. Date of Excess Allowance Auth. Headquaners {City) Total CoH _..3 9 _'.;,. less Advance I'/':,, cJO Reimbursement (<//, 05 Under penalties of perjury I certify this is a true and accurate state- ment of the city of lodging, expenses and allowances incurred in the- I have examined this reimbursement requC·st-and certify that it is ju,;1 services of the1Staie. ,, / 1 , . · • farlvvv-o (L Zfo--17" ~ . (CLAIMAN f ~" . (SUPERVISOR) ' Travel (~how each city'visited) 1 Transportation Subsistence Other E:s:penses Day from to I 1' !n-S1ate 0u1-of-S1ate l' In-State Out-of-Stale Explanai.ion Amount !>;& A'r t', ,: , L Jir,t_,, ,; t?Pr : R B -9,-~ qq ■-;£..,, . .;' 'h I II J-/1 . 'I A l i./.oD I 0 D ·7 ,7,:; ' Daily Private Car Mileage: @ c/rni1C p -H :/), co I Total t/3.'1< .;;,,_ -PP. h"c:.a1·~,1., i R B q ;;_ cc-11,.' /, 9,5 I. ',o.P,<-1. ! A L . jJ. ~ r, I 0 D - Daily Private Car Mileage: @ c/rni1C p H - I • ~ ~ Total "7 ,,:) _;;' I R B ■ I A L I 0 D Daily Private Car Mileage: @ c/rni!e p H I () ~ Total SI.VD ,, ,; 7 Mode of Tr~vcl: "(2JTrpc of· ·\ Tota\ Total Total Total Total R-Ren11\ Cu Sub1h1cnce In-Stale Out•of-Statc Transport. Transport. Auth. Subsist. Auth. Subsist. Other E): A-Air · Brea \;f 011 ~ 3.2S S 4.lS O-Other. r.i.il 01 bui lunch 4.00 i.oo P-Pr.-owncd car Dinnc1 I} 7 .7S 10.7S . S/oo J,77 Room .,. S .J-r,{XJ .Ji.. .J~:00 YI 42.00 sai.oo 1 I I I \'111i\l 1 tJIJ,1 EECt\?1 O 5 -0 6 -. ;.:; ;.) o ·1 -0 J 5 0 9 9 ◊ 0 :..:, i. .. i G •i CG -. -: · DEPARTilEN_T OF HUMA.N PJ:SUU Kt.,t.:, ·. ~ISION OF l!EALTH SERVICES . , ~UEST FOR OVERNIGHT ~VEL. ' I ... . I I 11 ' DATE OF LOCATION OF OVERNIGHT STAY (CITY) APPROVED BY APPROVAl ..... .. ! - = ' ... .. i I •• . I .. I I ' . · .. .. I ,. ! I I I S-c(Q)q /),, I WJ ' ~\ b/4\q:,1::, J t1 UL, \/00 ' I I J ('\)Y ' .. .. - I I i .. . .. , I .. I --- I ,I ' ' I .. ,· I , ' ' -I . i ' I I I I I ' .. I . ' 1- I -I I I I I .. I I ' I • I SITE INVESTIGATION DA·TE _______ _ I REPORTING PERIOD (MON~H) __ (YEAR) __ QTR. R.P. __ _ I EXPENSES: TRAVEL : DATE : ---,---To: __________ -'- . FOR: AMT; ---- TRAVEL TIME: --~~HRS./MIN. I ; . LAB DATA RECEIVED: DATE: _____ _ COST: ! ~-BACKGROUND SEARCHi . . I . I I ATTACH BREAKDOWN I . I I ADMINISTRATION -CODE]45: ------ l2Arr .· . . I . . IX. ADMINISTRATIVE REVIEW & DATA PROCESSING X. TY p E • Copy • Fr I E ! ' HOURS/TASK 5 HRS. 2:Coples -I for moln 11 le, I "' Ho.orked by JYBR. \)\ G:, I Gv.£ 'gc ' I. i I I INSPECTION DOCUM::NTATION (Sfo/f member) s I TE NA.YE fGX -Sf ft f f:JJ I LL E ID{ Ne}) o~s:L:/qR:c~ Site Investigation Dote for period covering ::::i-"1,(h to j lJU, (Month) <Doy) (Yeo;l. (Month) (Doy) I Expenses·: (City) Trove I: Dote: To: I ---- I I I. Backaround Search I I I I I. Prepore Study Pion i Sofetv PI an1 I I I:' rdlnote Site. Visit - I IV .• ·Conduct Field Work ' I ., ' ' V. Review Anolvtlcol Do+.o I i i I • Perform Ano lvses I I I I I I. Coool le, 8Yll I uate dzitzi, write re6ort ' I (Note whether. m·ops; Ice; 11 Im; etc.) $ Cost for trove! (frcxn expense repo.rt) ------- Dote Hours/Tosi --..... "t/31 l;:?hv -·. II I I ,Perform Hozord Rankl~a Svstem scx:;rlna <. SUPERVISOR REVIEW JA TE POSTED TO CR ~ g--0 \tt och Breakdown ind Telephone List • le· 0 /6/86 ' I ' I ,\ ' I 'I I I I Round off to neorest hour TOTAL HOURS ON SI 1::JM,D ' ' i - . --I. -0 L.IMINARY ASSESSMENT DOCUMENTATION SHEET -E NAME F C X ----cflu {uild/Ze. ID# ~F-EMBER ,//, /j,_((cuf() . GATHERING SITE INFORMATION .: . ! I 'I ' ; 'I I . REVIEW & EVALUATE DATA\ i ' V !.DRAFT PA REPORT i- JV LO o, ~ lf r &-s-;)_ 1 }Uk-._-- -, nATF /YR f-lRS /TAC,K (ii) ,;i./.z.c; ·'1 1/'30 If <:!,.,) 1-Z... 2.. 2/2.? (:I_) ?!:lo 11:~"' ,, /2. (3)2- ,< /2-><' :J.' 3°Q) Ii.'~ It I Z (V-1/ :,,_/z {, 2-'.' 3/;z... 1/, -·-'--------..,.......,--'------'-----'---..:._:___--1-__ _J_ ___ _ . SITE REVIEW MEETING. 1 PERVISOR RFVTFW ANn . r.nNr.ri:RRENC:f-" I ' MINISTRATION -CODE 45: 1 ·..., __ . TYPE' COPY AND FILE . I ~~ GENERAL ADMINISTRATION! & DATA PROCESSING .82B I I • ·1 I I ' I ,,_ j TOTAL HOURS ON PA: 29 3 HRS 2 HR ' i ·I. I SIT8 INSPECTION DOCUMENTATION SHEET ~ITE NAME Fcx-s\ma-:-;: v1L.,LE TEAM LEADER d 16~~-J1[}ay ~D# · l)lcj) CJ 9s,Y-.s-zs 2.. 7 ASSISTANr Q. JI/, cK ";__,roy. '· "-----------.------------------------·1 SITE INVESTIGATION DATE M/1-Y ), /9,fb I , REPORTING PERIOD (MO~TH)~ (YEAR) Jb 0TR. R.P. 4-- EXPENSES: I TRAVEL : DATE : s/4 -I s--/2,-To :_""'.-,/"'-'-Y.=4,=d,M'-=·=------ F o R : .. _• ------~J __ AMT:_,---__ i .1. T T 9.'_I' I -I RAVEL IME: __ .. _~_HRS. MIN. I I. LAB DATA.RECEIVED: DATE:_-_____ _ I posT: _____ _ I I BACKGROUND SEARCH 1 . DATE , ... s'-/2 -( .::i-/'-; ATTACH BREAKDOWN I I . I I I I ADMINISTRATION -CODE j45: .5 6' c;,;jr,, 6/21 e,/ Q..' (9 _;;-/,,,: ;;-/4,< . .,--;I,_'? {, 'i'. ·_ IX • ADMINISTRATIVE RdVIE'ri & DATA PROCESSING • • • I X> TVD, /':nDY .. f=°TI, ! ! HOURS/TASK I/ so C:, 1-1 R <: I I • ' / SITE NAME --~f_c_,,\ __ ~i _______ . ID# /IJcD a 'l's::y ,-,r [2.? ' .1 ~~~EPHONE CALLS ER~~ p~ ~R SI DOCUMENTATION l DAJ_J~ ____ _,_,TO,LL/.LFLl.>RO-'LML_ 1 .,_,( C,.,_,,Ocu.MLlP .11:LL_L_) ___ __1P_>-.U"""-L!N~O<J.LUT A..1o.Cc_i_T.,,,,ED,__ ___ _ ' . i/4-/< /4 C 4-,,¼.) ,1/ I H rf cLl 2 lo, r:ra •f ' I I I " I ' I I ' I -0 I . · 1 i I ' I I ! • Experises: ·I I ,os·T[D .I 0 SITE INSPECTION DOCUMcNTATION SHcET Hours worked ~y -~ P. ~/ (Stoff member) ' ' ' for period covering .i,.t.. Y , /CZft to 0,fl. 3.D, /");>,:.. I . ~ Woy) (Year) 0'i.bnftl) (Doy) (Yeor) I ' i s:1 TE NAME FCx fl~ I?' rte a C) ?o/S:SS 2 7 I ' ' s-/t/J(, Slte,lnvestlgotlon Dote ,7r/J'6 .:,.l...l.A:> .t'ULlll :>/ lj/tjb Trove I: Dote: .5'/4/4:e, To:. _ _z""-1 _,_t,,_,,cf:t:"'"'"''<c.1:tr:,:.;Le,,_· L<<'--$ Cost for trove I ( from expense report> ____ (include lTE Lob Doto Received ( If avol lob le ot:tlme of documenfotlonl: etc.) Dote: Round-off to Cost: ------:---~ I ., 1·. Background Search I I . I Prepare Study Plan ~ Safety Pi on -I 111. Coordlnote Site Visit - IV. Conduct Field Work I I V. Review Anolytlcol Doto I I VI. Perform Anolyses I _7,!;f ¥"~%; I ~ G1 I VI I. Compl le, evoluote d1'to, write report 7/g 1/9 I Q VI 11 .Perform Hozord Ronk I nq System '.seer I nq 7/<o I ' ADMINISTRATION -Code 45: Indirect Costs: I I IX. Administrative Review l D~t~ Pfocessing • Type, Copy, Fl le Attoch_Bre;kdown :·-·and Telephone List nearest hour Date Hours/Tosk -- (z)_(:f) 00 7//0 'll/1 1iL\-1/2,_ -'1" 3 .. / ✓ TOTAL HOURS·ON SI 5 hrs. ' ·- • Expens_e5;; . :· ,. " ' I • I. ' I SITE INSPECTIOll OOCUMC:NTATION S~EET I ~· "'""--'=~-"'~""-"'""""""'"""'"'°'_...,..,.-...,"""'9 Hours worked by r:/. /4);,,_,{./4,...___ (Stoff member) . j . . - . . for period co~erlng ,L .. -/ /, ~ to~7o , fr:G. I Cl,LL-.'-'L ---·,-· (~onth)<Day) (Year). l.\onth)<Day) (Year) I . IS I TE NA/-E 1101 M:l? !· I SIDS FODll 5/8/86 lab ·Travel: Date: (/4(ri. To:_ -7'i5~f.~Ji~~=~v_;~/~i?::~e-S Cost for travel ( from expense reportf~ Data Received (if voilable a't time of documentation): ·I (include rr etc.) Round-off to Date: ---,---- Cost: !· ____ I __ _ I I. Background Seorch i I • I Prepare· Study-P l_an l Sofety P,lan . -----·-·. ----· .. ' 111·. Coordinate Site Visit 1-),r.,/,N,-~ ,"3 O . I IV. . Conduct Field Work c;'/(c, /'is(.-;,.,:or, . . y. RevJ·ew Analytical Data I ' . ! YI. Perform Analyses £ /~-j ·--2 ."3o ; ' I Y 11. Compile, eva I uc:ite dtita, .....,rite_ r8p0rt I YI 11 .Pedorm Hazard Ronk Ing System1 Scor Ing i ' ADMINISTRATION -Code 45: Indirect Costs: i Admlnlstri3tlve Reviei( i Doto PrrOCessing Type, Copy, Fi le Attach Breakdown ·J I nearest hour Date Hours/Task -- • 5/C /gt, -:J :oo 3 . . c/"t/.or,-"!.' '3 tJ le, . 3 .. TOTAL HOURS ON SI I 5 hrs. ,2 Co?'les - I for mol n f I le, for = INSPECT I OH DOCUK::NT AT I ON s1TE NAY.:: RX-Sr,-,rc;sru .. L-E I DI NcJ? O?S: -1:SB 52 ::;z.. Site lnYesi"igotlon Dote f MltY f'f'l(_ for period coverlr,g L1/m · !rdflto Jt,,1,<.,f' 3('), /'lff . ·(f\onth) (Doy) (Yetr), (f\onthl (Doy) (Yeor) ~ ,::..:.-· /11 G --¢";~ Expenses~ I (CJt}l Travel: Dote: To: I ---- I I. Ccckground Se6rch I ' ; ! : Pr_epere Study P ! an I l Sei cty Pion I i ! ' oordi.nate Site Visit I ' -· I" '. Conduct Field Work I I ' \'. Review Ane!ytlcal Doto i V ! • Perform Anc:lyses I I VI I .. Co.':'tpi le, eva I u1:1te d1:1t1:1, write reoort '9 tJ t ' i (,.:/; - ' (Note ..... hether maps, ice, 11 Im; etc~) $ Cost for travel (from expense report) ------- DoTe Hours/Tosk -- .... l.'06 I t/;;,."1-4! ,~ \'111.Perfo,,; Hozord Ronklnq sy,ltem Storing /ti!.!, 'L),., J '; $ ~ """' : ~/2c-4:,o c/.:u. • :5 • ~o / 2: j'O X. SUPERVISOR REVIEW 21-,E POSTED TO CR__{)! :29; 8-.7 r.--;-t c:.ch Breakdo'"'n •nd Telephone List :C,e-~/6/86 I I I r I l i I , . /3%-/ Round off to neerest hot.'r TOTAL HOURS ON SI Site Name • I TELEPHONE TO/FROM (COMPANY)· I . I ' ' ID# A/CD tJ"/5 -'1585;,__-:;- CALLS (For PA or SI Documentatio=] PERSON CONTACTED \ V c· :.C?·les -I for moln fl le, I for I ,j INSPECTION DOCUK::NTATIC>:i period covering /4,,, L, ft to $0 "3 I, . _,_(~Doy) .• (Yeorl. •.. (Month) (Doy) I :: xpenses: • SITE NA!.\E Fc.x-si-~4,.::, 11., ID/ ,,{/C.D O<fS +;Ff? 52?- S lte Invest igotion Dote b /11 Travel: Dote: (City) To: I (Note whether mops, lee, 11 !m; etc:) $ Cost for trove I ( froo expense report) ::::.~=v· - ! I '=.c.c'r~s;,ou,1d search I ' I :: :-~;,=.:-e S7udy Pl en I, Sc~ety Pieri ... I •--c• ,--: ~·-. ';-i ... 'C: Si 7e Visit ' I .:.C:1ci~c7 f"!e!d Work I I ' ?.evie .... · Ane!vtical Deto I ' Perfom Anclyses i I '. j. Co.-:ipl le:, evalucte dota, ~rite report ( I'> M«A--g;:f'i) (1q r,'\,"-4, -.,. : 0 C>) (;,.o MC.;..~5:,o) \'I I I .Perform Hazord Ronk\nq Y. • SUPERVISffi REVIEW ~ 7'":" e.Ch Breokdo°"'n ca~ Telephone List '·• ~/6/86 System I • .Scor\ ng I I. I I . I I Round off to ------- Date hours/Tcsk -- I /9 :4~ '. /'j nearest ho"ur TOTAL HOURS ON SI ~ ' ' 2 Coples - I for main fl le, I = worked by C. µ,-, t, <--lj .,\..,.-. I I for per I od cover Ing /l,,r. / / , 1.1_ to . ___ rnbnth) (Doy) .. (Year,.). ' I INSPECTION DOCUMENTATION (Staff member) • snE NAME FC.x-51-,,.k-s;-,11~ IDf PC.b C,?5' f:_!;E:, :5J.."'1 Site Investigation Dote 6 M. Expense,~:., .· .. (Cit~) (Note whether mops, ice, fl Im, etc:) Travel: Dote: ____ To: __ ' _______ $ Cost for travel (from expense report) _______ -'-- I Date --I I _. Background ~earch I I '' Pr~pa~e Study Plan b. Safety Plan ''. ' _:._~oordi.nate Site _Visit I I I I y. Conduct Fie Id \fork ' ' \'. Review Analvtica! Data I I VI, Perform Analyses I VI I. Como I le, e Ya I u ate data, write I (-f-"> / ;2 '. 1<>) (-f-'/ I :oo) (4-'l{S.:1¢) {_4.'i,~; ct.>) r~port (4-i3/;,:u.,"\ (-,-n-/,.,,4~)(1--21/1 :oo) · I . I YI I I .Perform Ho20rd Ranklnq System Scoring (,$/ I !Jo) (4.,,,1 I'. IF) (4-ll '/z :u,) (i--n/1 :«.) X. SUPERVISOR REVIEW i-.tt~ch Breakdown end Teleph6ne List ~ 8/6/86 ! I I I Round off to nearest hour TOTAL HOURS ON SI Hours/Task . 10:+5 . 5:-f5 I:} • I ' I CE NAME ~t: c_ )( -✓f~JP& ID#_~),:....c."t_,tl_--=:.._· ----- ! TELEPHONE CALLS (FOR PA OR SI DocuMENTATION) TO/FROM ~COMPANY) PERSON CONTACTED c2 X ~ ld£Cri-= F D I} z..._ /.11-l I ' . 'I ., . I 'I ' I -1 I . ! I -' I,: :/ ,. • --2 Cop"les - I for moln ii le, I for = . I Hours worked by C,/LM/(fl.. !U,u-tC-Lfov · I I I .I I INSPECTIOI! DOCUMENTATION (Stoff member) SITE NAME FCx'-51-.,:./.,,,,.,,.: l/c I DI ,UC-7) 0 75 </-_5'"{J S-z-? Site lr.vestigetlon Dote i, fau,.; 'i[t th~ .. , {,; ;,~;,,-} 1 .2 -bo,) J1r./4"A CT>-".-(t./23/g,.,:$ 2£t2)(t_/2';1rt -d1P_) • Expenser,.:.-.• 1 • -- (City) Travel: Date: To: $ Cost tor travel ------~------- ' I ! I. Backqround Search I I ' ! !·. Prepare Study Plan l Sofety Pla'n I. Coordinate Site Visit - 11'. Conduct Field Work I' . Review Analvt\cal Data y I. Perform Ana I yses Yl I . Comp I le, eve I uc:ite data, il'i-lte VI I I .Perform Hazord Ronk I nq System X. SUPERVISOR REVIEW DA TE POSTED TO· CR -~_/Jd 1f] -Attach Breakdown and Teleph6ne List • • Rr ·_ . 8/ 6/B6 \_ _-. ' i I ' I ' I I I I I I report i I Scorl ng I i I I I ' I I .\ I I. Round off to nearest hour (Note whether mops, Ice, film; etc:) (frcxn expense report) ------- Date Hours/T llSk --.... . TOTAL HOURS ON SI ~ • ---· -----_•--·--_ . ..:...--~-----------------, i -..:v; iii Vcit viii Id Lit::f.Jdi ti i lt:i fl Ui Ii i::ii ISµUi li:iliUii R.ODUCTION WORKORDE.R-HIGHWAY PRINT SHOP •. 4-20 -'();i-Dept No W,11,4,1_} QES Date Project No. Order No. _______ _ TYPE OF REPRODUCTION PHOTOCOPY: D Xerox 9400 OFFSET: 0 Multilith 1250 Phone No. 1:5> -Zi5 () I Room No. ~/3 :BATH Auth.1f = {J;L~ D Xerox 7080 0 Multilith 1850 S GNATURE / Merox 2080 /·'l'vellum) ., WET: □-Amm_:n~ · _____ ?_~r~~:1--A-______ -;-_________ 1_ '--------...,._ -----Masters:-Forms;-----~ront & ant . Tracings. etc. Z. No. of Copies { □ · Back --:;7nly I • {NUMBER SIDES) y.~'\,I COPY SIZE: Sheets O 8½X11 D 8½X14 0 12X19 D 24X36 0 Other Rolls D 18X_ j>(·24x~ 0 36X_ 0 42X_ O Other PAPER: }¥z_.Plain D Bond LJ Blue•line D Sepia INKS: ~/ "'Black 0 Red \ 0 Violet 0 Other HANDLING: D Collate □ C!S D Normal D Punch D Cut D Onion 0 Vellum D Yellow 0 Rush D Staple 0 Fold D Color D Green □ C/P/S D C/F D Letterhead 0 Blue D C/P 0 Bind Special Instructions: z . tuA ;9,--v;2 , / -f-21-<??--~;zr,;rx C!o~ /. ;e,,2 "'0 7o.,..,,,; L JC,... t C,,aL, F/4tu I.. FCX-6~0& ~£//= :,z~ ~~~ • • ----------·--·--------------------:l ., " • '(~~;. ~ -~-1:~: ·--~--_::... _.,._,) RAlEIGII BlUE PRINTERS Blue Line Prints: Intermediates, Engineering Supplies Maps (Agents for US.G.S. Maps and Nautical Charts) 313 W. Martin Street• Raleigh, North Carolina 27601 e (919) 832-2841 .1 l cusTOMER Gr2ovc: ;·2 N •CHOL-~-c 1,.J DATE-<f/(r:-/8"?--. I I ADDRESS 2w v ,re.ow . /-(en c:r 1-1 S-cc'r: ,,:._j Cs Q(' ,L.A {) 1-J \ 1 . . .. _ ----Rrf\ z..o 3. [2,A,H f L;Qs_ ---A-T-TN .--TEf2L'sA 'BRXJK'.::5-----~--'"-' ~ • _,,.... __ ,.. ·"' ! In --( l ~ C7 -~><_.. FC-Y-5-id,..,, .;, //,, -/2.t:,D Fu:-w~k.,., /--.,-c-..-C:._.-; D / I , --:-_/' /l ) -/-t1 I l__,,,f-; ~ I V ~r...1 S-,_.., I , I • DELIVER □ w~\"12-I rf oc . ,y.,\ST AL . PICKUP □ , r:-Si''' -~ 'fl\\_\ , < ??-' t-~ s c;r: \_t-\\S--~i'-1 TAX □ '?. -·\_'\ ':, MAIL ,_,,ci~\ '\. i,11f\\\_t-ll, "I) l:,t-TRANS. TRACING RETURNED□ 3810 /cf -. r'' -/•J TOTAL , \ CUSTOMER • -------~""----f u • Form No. 1034 Rev. 9/85 .. J-· • :) ·, North Carolina Department of Transportation REPRODUCTION WORKORDER-HIGHWAY PRINT SHOP Date -"/-/5-8-+ Project No. Order No. ~------TYPE OF REPRODUCTION Dept. No .. /4 . ) . / . ., . . . .,-,/ /,-1. tL,,;. <... k1 /! t::"Z-0 C.,g,/.J Phone No. /:t ?-?-Zu I Room No. !? > ~:' · __. Auth. 1<>;,c,.._ _ / SIGNATURE .·_.: ·----. _!'_'.'OT~C~Pt ~□ :x~o}9~QQ__ ~-~ D ),e;_ox]OBO-,--~ □ 10~~1~~1so.-JJ{})i: OFFSET:. 0 Multilith 1250. D Multilitli 1850. . •.. . . WET: 0 °Ammonia O Mirco-Film . ·: Masters, Forms, . / . Z,.c Front & :hFront . Tracings, etc. · · · No. of Copies · D Back . Only_ •· (NUMBER SIDES) . . · · .... COPY SIZE: · Sheets Rolls o sv;x, 1 D 18X D 8'/2X14 D 12X19 PAPER: ~Plain . lJ Blue-line ~4X Z-4 . □ 36X ·o Bond D Onion D Sepia 0 Vellum D Red D Yellow INKS: ¢( Black 0 Violet. · 0 Olher HANDLING: . D .Normal 0 Collate · D .Punch. · □ C!S □.Cut D Rush D Staple. · D Fold Special Instructions'. · ./{,(!// 12-,,J D 24X36 0 Other · D 42X __ □ OIiier D Color D Letterhead D Green D Blue D C/P/S. D C/F •••••• D CIP . .': ,• · :0 Bin·d · VP > 1'-'/1'-'fl? . I Fe. ;I-9,,, k;:,/; //4 1t?j1,~ 65/-= ?g~ • "'· . • • • I Form No. 1034 Rev. 9/85 North C*rolina Department of Transportation.· REPRODUCTION WORKORDER-HIGHWAY PRINT SHOP ' Date 29 7V.,ut ? l Dept No. t-/4,dJ./L,v1 f!ua_ Project No. Order No. ---.---- TYPE OF REPRODUCTION ·I ' PHOTOCOPY: 0 Xerox 9400 I , OFFSET: D Multilith 1250 ' WET: 0 A~monia Phone No._~i_-;_,,~7_-_·. ~C~6'_0-'--/ __ Room No. Z I 3 i3o fC.. Auth. a,,~µJc/4--_ 7-SIGNATURjt · D Xerox 840 ~erox2080 0 Mullilith 1850 D Mirco-Film Masters, Forms, /j / Front & fa(:Front Tracings, etc.--~· __ No. of Copies __ -'--□ Back Only (NUMBER,SIDES) COPY SIZE: Sheets D i 8½X1·1 D 8'/,X14 D 12X19 D 24X36 D Other Rolls .I D 18X __ '.-· □A4x_{j-D 36X_ D 42X_ D Other PAPER: ~Plain I D Bond· ! lJ Blue-line • D Sepia INKS: ~lack I D Red I D Violet I D Other HANDLING: 0 Normal I 0 Collate O _Punch I D C/S · D Cut I , I D Onion D Vellum D Yellow D Rush D Staple D Fold D Color D Green D C/P/S D C/F D Letterhead 0 Blue 0 C/P 0 Bind Special Instructions:.--~--------------- . U/4 I &.c2. -V 12 J' 0 J (/n,.£ 7 / I I ,I i I ,. I ' • I 7 Co?ies -I for ~eln fl le, I for\ doto P' . • 1 -·\ I TE INSPECT I ON DOCUl,:C:NTAT I ON ,.,., J, i ' . Hours ~orked by 6eoJ./E ,e_ /V ICH {J L ~ o N (Stc::ff--nem!)er) \ I I for period covering. 7t,JLY -/ , .13__ to (Honth)(Doyl (Y,arl ' Expenses:··· 5cP .IQ_, :S:t:: (1-\onthl <Day) (Year) SITE Nl\'-\c Fc,y-:Sf-,./es v",//.,,_· IDf A/CD cJ'/5 158 52.?- Site Investigation Dote -1-IJ7/Jj (City) (Note ' whether@lce, fl Im, etc.) Travel: Date: ____ To:. _ __,~ _______ $ Cost for travel (frcm expense report)_..,/-=..c,_o~-____ _ Dote Hours/"f ""' I -- I • Background Search I . - . . I II. . Prepare Study PI an & Sofetv Pion • Coordinate S;te Visit I I I .. IV: Conduct Field Work I I ; V. ·Review Ana I vtl ca I I Datc1 I I I VI. Perform Ano I vses I i VII. Co:nol le, eva I uote doto, 1<r!te reoort ·-• I Vi I I .Perform Hazard Ronk I no Svstem· Scorl no 4u;u 6 ".S. /21-z;-;--) /r /77 -i? ,c,) x, SUPERVISOR REVIEW - DATE POSTED TO CR _j_;JO 1.Jf__) Attach 3reckdo~n ~nd Tele~hone List • . 8/6/86 I I ' ' -; . ' Round off to nea.rest hour TOT Al HOURS O,~ SI I I /!'E. z. . Site Name ID# NC..l)t}C/5 4S-'il sz+ TELEPHONE CALLS (For PA or SI Documentatio~] TO/FROM (COMPAN~) · PERSON CONTACTED C,v / CJ, ? ""-b 0-A-0 -e,/:rd(L X/; c ho/4 ""'-/4 I I . ! I I .. I I • • 2 C'.l')p!es -I for main fl le, 1 for INSPECTION OOCUMcNTATION Hours worked by G,e:o vef2. N1c.t1lo L..$0 ..J (Staff member) for per lod I covering Ocr · /, ..:JiL... to (Month)(Doyl (Year) I Expenses:.·-· I (Cit/l I. 11. Trove I: Dote: To: \ ---- Background Search .I I ' I i I ' I Prepore Study Pion l Sofety Plan • Coordlnat~ Site Visit I I I I I ·IV: Conduct Field Work I I y. Review Analytlcol Data i ' I YI. Perfonn Ana! vses ' I Y 11. Comp I le, · evo I uote data, write reciort I pee. s / ' 8'1--~--(Month)(Doy) (Yeor) SITE NA-~E Fc_x-.iTAT~su, LLE I 0# MC p C!J:S -1-5{] 521 Site Investigation Dote :;z_ /I/Aft[(, (Note whether maps~ Ice, tl!m; etc.) $ Cost for trove I (from expense report) J/,,-.,,..z Date Hours/Task --·--. -·. YI I I .Perform Hozord Ronk Ing System Scorl ng AvPtnovA-l..: (,i/;1/n-1 ~J ( !!. X. SUPERVISOR REVIEW DATE POSTED TO CR /'l7~_1f] Attach Breakdown I Telephone List R 8/6/86 I I I i I ' I . I ' · 1 i I I I Round off to nearest hour TOTAL HOURS ON SI I • . · ID# ,UC.[) ~95 ?S.!J 5"29 TELEPHONE CALLS (FOR PA OR SI DOCUMENTATION) TO/FROM i(COMPANYl PERSON CONTACTED I I ' . i I I i . • I • • I. ·:· Pn::rT[U: I • • • R:n: LB= fix H:urs & M::nies "fBll:_ AFiffi SI (HR3) rEjXrt rraiJ.e:1. to EPA. ! &fI.OiEES N\'E G f2crVE /2 /l/, CH "L. ~ 0 ,J . RBI'ITCN be O t..Ot; I .S [: ., Sl'IE N"t£ kX -$ r ,-,. rc'S v t <. I...<;'" . EPA IDJ /v(D 695 :95'8 52'7'- Field I=tig3.tio1 [ate ______ _ IXDMNI!mCN KR QJ\RfER CDlERIIB~M L,ltt&_ to Mar -;3_1__, ~ ! ' ( )(i:ay) ~(YEai:-r~ (M::rthJ(EayJ (YarrJ (N::te: Olly Q-e (1) SI D:o.nalf:aticn 8u2t fEl'. r:ers:n, i=er site, i=er qnrter I , . ..,_,. ~ lNJ.ffi!D m aro.e site cl.n:irg staw OBrter, -- 3rn -rn-a-ate Tcansp:lctatim $___ _3ll2 -In-Btate &l:sist:e:= $ _ 3121 -OL-B:ate 'TI:ansj?xtatim$___ 3122 -Qt:---8@1:e &i::Eista=$ __ _ -Ice I $ -1'Bp; $ -Film : ' $___ -Cti= (List) ___ $ __ _ H33JJ:h & S3futy ~ ( if U93:l) : • , I • · -R=iirata:s · , · f . Oii:er -~ I f Ctrer ----- Icil I a,,1, , y S'iqiles ~ ·N.ni:er of ln:Jrg3nics 83nple:1 I N..nter of 0:g3ni.cs S3np1e:1 --- !UR, JNXRID L · ~ &-ai:ch i II. PrEf&l'.e Stlily Plan & Sifety Pim III. Cb:xdirate Site Vi.sit N. Chd:ct Field W:x:k l\:::tu,)_ hrs . in field Tr:a\cl 'line to arrl fran site V. ~(3;{ kalytical 03!:a I VI. Eerfmn ~ . I _ VIII.Eerfmn Imard l«ki_rg Sys1:an 8:ari.r}3' x_ .SJPEMS::R R8lilW ' I . , (R:u:d off to rmrESt J:u.n:) 'lOJAL 1:UR3 CN SI . . ;: ~~~ rAIB KSlID 'lD CR _J/ _lli ( --. . fb..rrs/Ia3k: I I __ HS I HRS I I ( . Atta::h &ool<d:i-.-1 ifit;;;;;;~~ifi~;;~~tl~~fi;'.~~~~~~. ::~:i~II~\ r 'I : , I • -· •• ·' DATE: 1 August 1989 TO: File I FROM: Pat DeRosa~ RE: FCX Statesville NCD 095 458 527 On August 1, 1989, I spoke by telephone with Don Rigger, EPA OSC, FCX Stateville regarding the scheduled installation and sampling of additional monitoring wells at the subject site. Mr. Rigger said that EPA will be installing 2 sets of monitoring wells at 2 locations ' at the site beginning Monday August 7, 1989. These locations are marked approximately on the attached map. Well construction, development, and sampling will probably continue throughout next week. The 4 MW' s c:urrently on1 site will also be resampled. The new wells will be temporary, cons1tructed of PVC. The shallow wells will be cased down to bedrock (iiliout 50'} with the screen at the bottom 10'. . ' The deep wells will be cased to hard rock and open hole down to about 200 1 • Well A will be located outside the NE c:orner of the building. The purpose is to get a '.handle on groundwater flow and gradient. EPA is trying to determine whether ground water is flowing to the east or ' south. A~so, there are currently no bedrock wells at the site. ' Well B will be lobated about 20-25' east of MW-3 already on site. MW-3 has shown lindane contamination. The purpose of the new well is to determine whether contaminants have moved east. ' S3.Illples will be analyzed for a full pesticide scan and possibly ~hlorir.ated solvents. Don Rigger can be reached this week at :912) 964-8016. Next week he will be staying at the Hampton Inn in Stateville. Attachment PD/db/FCXSTATE.PD II I Contamination Summary ... LI_, _v .,,_ ,,., , " -,---------11 / /,,., , --- / 6-C Tar Dist./.,&, ~- __ Ba!?.t /tJGT:PV .. : :Yiv[)lt~~R. ,r::;, C/Ji:'(/f'TIO}) /v/lL/( CO ·' I ! I .. I··• (I\W 1" /+" ·-. -1-.. I f / · Carnation Well Cl Solvents I I 1. i . / I / ' I / / r i- 0 i I I_ __ __; / 0 s P -Sv"..f:1<(..t! ~,.r-cR.. ORA ,,J. M YI-l'-M·/.'r Toi?.. v,,/£"!...l- F P -Fu:::. ;~..,A,f<-, :..;~ ·::. FCX Statesville(NCD095458527) & Environs--Soil and Groundwater Sample Locations \l ~\. " /\ //1 ----------------------- - - -· DATE: ,, ·.: ,l m;ITED Srt.n:s EW.'IR.O!l)Q;J,'TAL PR.OTEC!ION AG!cNCY' REGION IV 345 Courtland Street, N,E, ATI..A.,'TA, GA 30308 FACSIKILE TUNSHISSlON SB.EET q///?41r. ~ I(!) /i::5 ~1.JKBER OF PAGES: _ _J (IncluGed Co..-er Sheet) --'--'-.;..c--'---'-------=----- ADDRESS: FR0H: If the fdloi.·<.::.; m•ssage is received poorly, Please call ---------1 p c;i~ ,.::ice ,.t ?TS 257-or commercial (404) 347---------- SP ~C; AL INSTc'.,:CT I O!lS : _ _c5,_"":::;{?_~/...c.e._;t, .. o_/ ,/ ___ • --;1--+;-'-'-'~ht..<,o___,'--"---~--'-==..,V-=--- ,.l,<.A-/~. a.., ~ ~ /215,;u... zo ~_'67.· PLEASE ln:rlll I!: R ALL PAGES REGIO~A.L OFFICE FAY. NUMBcR: FTS 257-44e6 (AUTO) coH:M'. (401,) JO-i.486 YTS 257-4702 CG:-1.: .. :~ (4(,.,) 3:.7-.. 7~,~ I I I I ' j I l i A I I <::, NC I J. ! V1 :,: ,;-./ i ~ 0 ,-I ~ I i ' ' \ ------------ , . M 1d 2 5 )~ eJl J l..._ ~ C /, l r i. c,~ To,,~ L 1 J j -·G i c~ le r0 e '1t, UN!_ j j_ -I); c.lJoro eli7 l,._,__ (1 ~ -~1 i,cs, C /., f o I': cl, /ejr ~(fo,oet(1 L,~ j_ J 2 -T f' icJ /c r,...' e f io. ,-v-1 I ) -1 ·r, J / olq :etll i_,,_,.._,_ T:c, TR L.. f1 e_ +~ { 4 ~ c ~ / a I', ul c/4 toro '6 r- I , I '2. '-I ;2. 08 /vlw3 (Mwz.J Mw rf (M(0lJ t1\A!) (H GJ 31-t) I 1 1 -D i ch IO r O C +i.cv'IJ,_ !'/ 3 f'/'j I I J' I i 1 -o,c4 D1Qc,J,7Gr~ /'-, {., / _; ,n.P ✓ __!_. _J !/, & I e , /'CA cl_ / o roe_ t , J ,ui J). l ft"!, 1 i i -Tr , cl/ o oe J/aAJ2 /0 '3 f'/n6 ) I . Tr; c_ /,, / o ke. ¾/ ( ,v. , l 9 o r1/; Tl',·c i fore, r.lvO/cJtJ•'L/li,u 7 '5) /7,:,,"f cliloroC:irM (J , 15.'J 1y; ToT/.!L J. /IJ I c,/,/o I~ J/0.n_L /· 7/ 1 :J I' · , ~ / // G IS-o I -,....)1C. O(C·t/\7 .-"' 1'1 e fh / ~i\J c A , o r u~ '7 ~. A • )() 1e1/ ,c, c( loro 12J(1 t.2,0. 82' ' i 1 .1 l -I r ,ci lo f,::,e/J,c.,,~ 5'.27 I -( j/ 0.5 5 JI J. 1 2 -.Ir ic~ u r o .q 1 (c, A.Ii (.., ' Tr , c / { o r-o e {{ J ~ ,,\.Q 2 '.;It . I -c~ lo roCa rh J .£ 8 iJ ril;. -B~c -5' be~-DHC 7f ,,;-. 6aJ" l'/u. -E )/ c '25' . ; -AL (/ · · ~ -I · ti, ) c I ·· · . (:) 5 r:c ) .,., C 1C "5. !V/c: 1ll, t.~ Ci I~ (•1C~t ;? . t,) 1e_ ~re c4 ~ r~~ 'K/ G rV. /.O/ &ie--BJ!c !06 le:; 1 /!.. L ( (,. 5; oc 5 /c;,G 1 ) ,. ,, . I , ! /Jf;_(,3 :!_oo. 52 j (, ( ! (o ( ~ c,v, 7 t' /~c c J IQ r ,J.,, Me..µ 7 l I'(,? c: Jj_,.~,i.l!o 111; J -7r' ;cl~ 1 uc?!Jo r.y 11 /c.) /4,.:, {'luop-c,"V!.//:vy_ cL!oruG,r,., 'ioT/)L 7 88 /_ 83 e ao 7(,7 DI\TE: TO: FROM: RE: 8 June 1989 File ( Grover Nicho\son tJ;f'/) d, { Telecon w.ith br. /Jdo, Environmental Epidemiology FCX-Statesvil;le Sampling T spoke with Dr. ~udo today about the stream and well samples taken near the FCX-Statesville site on 27 April 89. The well sample showed only a "trace" of! chlordane. The stream sample showed < 1 ug/1 trichloroethylene and 4.6 ug/1 tetrachloroethene. All of these levels are below MCLs and are n?t hazardous. ., I . . -I. . ._ .. Nor:th Ce.r:o_li_na_ Dopm::tment of Hu.rn:e.n Resour:cJl!r_:_o·c-c·: ·E,·v·: E·. ·o···· ·.--. / ,Di vision of !loo.1th Ser:vices · .. _, ; _ _f\&;;.' · , ,' I' Labor:ator:y Section · · _ _-. · .:· 11 -· · · · . .-... P.o; Box 28047, Raleit;h, N.C. 276ll .· -·mAY 181989_ >. En,)ir:oomental Scioncoo Analysis Ropor:t s~~~#l@lllllj}J\MCH ! 401 OBERLIN RO,'.\U I Addr:ess:_;:~u.,::p:...,...;f:t.,~~':f:.~g..,'-"'2ff!d . ~ { , , { l - - { f _ County:_'1=£..~~4-L-hL~~&~~-f>-<c-----,- Ropor:t to :'.£!:_::1/Zd..l~,?/it.~'?~l.¢d:f1"!-:::J__!___ Addr:ess:~~~~~~~~~'f1--;f----;,----;:;,;? o,i, c,nooeo~---~• Collected By: _,di;_____!__ ✓ : Analysis Desir:ed: ./ ' I Labor:ator:y Slllllple ' Srunplo Descr:iption or: Reraar:k.s Results In I Ht.trJber: Nurober <?'l11'-4 I ,:, .. __ t .. I I I I I I ' ' ! I I I : I I ' I I I I Date Received gs-;-r'9, I V-:> . I Date Extracted 5-f-.f'?YeM~~ Btv~ ; S'-'9-'i:9 o\8,ll.o.,Yli.J I OHS Form 2364 Revised Labor:atocy (l/87 li I I SEE ATTACHED SH~l:S) SUPERFUND BRAN"CH ... - 4U1 U~t.h.L.11\l l\vn- ., .. ;,iWJ- <;,).J.!8'9(Ll Date Reported s--;t/-tf '\[CC.. loa ~c'JTLE,f:. ·-K-'llif._;,fl' Date Analyzed ~r, _ ,.,_, _ -:l-,,;7 v"' "14 · -1'.- Repor:ted By: I /4.&:Jh ,f';J/1.,,/ ,r_,,C.- (Y Kildced A. Ke'rbai.q;h · Dir:ectoc 03V fJO:.ii) t) eaer 8 l YAM H3"AA8 O~UlUltJt • .. C. Dcp:ir~cnt"of Human Resources ,isio~ o( ::-ic..~th-Se-rvices e Number me of.Site lleaed By __ Groundwater (1) _. _ Surface Water (2) --Soil (3) __ Other (4) INORGANIC CHEMISTRY G; jq, ve R.. t0 , CH.<:> c.... ~e -...J D\JPc'RF\)ISJ:) ~f"t~CJ,f Extractablcs ' I Parameter Rcsulo; mg/1 ' Parameter I ._Arsenic _I_Ar.enic _Barium _,_Barium _.Cadmium _l_eaclmium _Chromium ,, _._Chloride _Lead _i_ Chromium _Mercury _!_Copper Selenium _I_ Fluoride ..-.....;_, __ . - I 'I . -------__ ilon _I Lead _I_. Manganese I . __ . Mercury __ i Nitrate __ ! Scleni~ I Total Rcsulo; mg/1 Parameter Rcsulumg/1 __ Silver __ Sulfates __ Zinc _Ph I __ Conductivity ! _ms -, .. .... _ .•. -··-. .· . _____ TOC ORGANIC CHEMISTRY Parameter Results mg/1 \Parameter Rcoulu mg/1 Parameter Results mg/1 _P&T:GC/MS __ I EDB ...L-Mcthoxychlor ""<CQ,OQL ~ Acid:B/N &$EE ATTACHED SHEET($) ' ~ Toxaphcne __ , PCB's ""'Q,O0ib _TOX __ ; Perroleum ~2,4-D <-0.00 I -~Endrin < Q, 000/._ L Z;t;5-TP (,ilvcx) <O.C(17 --2:.JLlndane -C:::Q,{200~ ~ ~Dt <Q-'212el.. 'I. ;"11 ;-,. k! r"i " <=°,?, 00 0 / V ()(.I ' ...D • 0.000.:2._ ,;f • n MICROBIOLOGY ! RADIOCHEMlSTR 1( 7,<?,,ic,::: A r>1,:,, ,,7 Parameter I P 2ra..ID. et e~ Rcsulu PCi/ 1 ~ '=' ; ' \ .. _ (MF) Coliform Colonics/JOOmls __ Gross Alpha ' _ (MPN) Coliform Coloni...s/JOOmls __ Gross &ra I -' -- ' ---I I I : Recci vcd -:7--;-,-----;,FE.t;.,,--...,S""S7 __ ---.,.!----- ;/0..b ' 5 I = I "' : Extracted 5/'J../'8'1 fL.) J --17 71'.'.s'. ·Pit{, CTW orrcd By I J\OJ (R.(',·ii..::d i/85) ~~ I L.: •••• -1-..• \YI ••• _ to_ .. ; ___ .~ /Q-,\ C. D~ r.:,1t::nt or" Human Roources vision of .H.;.,lth Services I • -. $A~PLE ANALYSES REQUEST I State Laboratory of PubLlc He,lth P. 0. Box 28047 306 N. Wilmington S:::-cct Raleigh.27611 :e Numoo ·NCD I Q95 %:8 52.'7- ,llecred By di~ --JiwJ \ Iff-----Date Collected -+--~......t..-.lL...,L..,'-,---,- 1meof.Site fi<~)(--S ~res l")~L-1: ···.s.teJ.,oci;:io:o 'pc ofSampl: ~ ~~ ~ ;;}-j C :;J__ Environmental Concentrate Comments I --Groundwater (1) __ Solie! (5) I . ~-Surface Water (2) __ Liquid (6) ,, --Soil (3) __ Other (4) ' __ Sludge (7) I __ Other (8) \ 1>r Vo A. I I I . INORGANIC G'HEMISTRY CC.·. b e.o Ii eR. N u:.H.o L-!:>t>t.J Su I>-~ FU~D "°?~A'l-)C.t/ Extract:ables Parameter Rau!t&mg/1 _Arsenic _Barium _.Cadmium _Chromium _Lead _Mercury ___ Selenium -·--. --·-_Silver ----- Parameter· Resulu mg/1 · . X P& T:GC/M!S.t P.TTACl:lEO e1:1Eft(S} _ Acid:B/N Ext. _TOX MICROBIOLOGY Parameter _ (MF) Coliform Colonics/lOOmls _ (MPN) Coliform Colonics/lOOmls I I Pan.meter Results mg/1 I _!_Arsenic _!_Barium _;_Cadmium I _,_·_Chloride _1 _ Chromium I __ Copper -I . . .-_. __ Fluonde -··-·-·-· ; :1 • __ Iron _.I_Lcad _I_ Manganese _I_ Mercury · _I_ Nitr.a.te. _I_ Selenium I ORGANIC CHEMISTRY . : Parameter ' _I EDB _I_PCB's --J-Petroleum -2:,_Endrin LLlndane /( -n,e Id .-i" Resulu mg/1 Par.mete~ __ Gross Alpha __ Gross Beta Total Parameter __ Silver __ Sulfates __ Zinc _Ph __ Conductivity __ ms _: __ Toe -- -- ----- -- -- Pan.meter _¼_ Methoxychlor LTox.aphcne ~2.4-D Rcaulumg/1 Results mgll L2,4.5-TP (,ilvcx) ______ _ ..lS_ l?:PT y... ri..t--.J-"~ RADIOCHEMJSTRY Rc.ulu PCi/1 te Recc::ivc;d -------------'------Date Reporred -----:---------------- «Extracted------------'.--'-----Oare Anal\=d ----------~------- ported By --------------'\'-------bb Number S 3101 /R,;~·1Kd 7185) .1 ::..-..l H,-,,.,1,..,1~ w~ ..... (R,.,,;,....,_. "i!R7\ BASE/NEUTRAL AND ACID EXTRACT ABLES COMPOUND N-nitrosodimethvlamine bis(2-<:hloroethvllether 2-<:hlor=henol phenol 1.3-<lichlorobenzene l,4-dichlorobenzene 1.2-<lichlorobenzene bis/2-<:hloroi llether hexachloroethane N-ni troso-<li -n~.-.v,v]ami ne n i trobenzene ; 'vV"'lhorone 2-nitroohenol 2.4-<limethvlohenol bis<2-<:hloroethoxvlmethane 2.4-<lichloroohenol 1 2 4-trichlorobenzene Mnhthalene hexachlorobutadiene 4-<:hloro~resol hexachlorocvclnn<>ntadiene 2,4 6-trichlo....,..,henol 2-<:hloron>nhthalene acen•nhthvlene dimethvl ohthalate 2 6-<linitrotoluene acenaohthene 2 4-<linit....,..,henol 2.4-<linitrotoluene 4-n i trooheno 1 fluorene 4-<:h 1 oroohenv 1 ohenv 1 ether diethvl ohthalate 4.6-<lini tro-o-cresol diohenvlamine azobenzene 4-brnrr.nhenv 1 ohenv 1 ether hexachlorobenzene =ntachloroohenol ohenanthrene anthraceoe dibutvl ohthalate fl uoranthene • I STATE LABORATORY Of PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. OEPARTl1ENT Of HUMAN RESOURCES P.O. BOX'\28O47 -306 N. WILHINGTON, ST., RALEIGH, N.C. 27611 : I . I ORGANIC CHEMICAL ANALYSIS LAB NO! FIELD II TYPE I UNITS I /(\/?2A I ' I I I I I ' I ' I , sa?N ... <fo '" -'"O ",Ql ~"O IO• '"30 ,I/ '>0, ,,,_c-,, ', ,,, ·,30 ,,,1::1,~ so/16.SC 1,,/ ::,::,,- ,, n,, ,,.w ( l .. n;J),~ I .1 . ' I ' i I I I ' ' i ' ' I I I I ' ' I ' ! ' I ' ' i I ' I ' I . / ( ) ( l ( l ua/1 ua/ka ,m/ 1 .. n/ka .. n/ 1 .. n/ka J -Estimated value. H,.o/SO/L-I\ K -Actual value is known to be less than value given. ( l .. n/1 ""/ka L -Actual value is known to be greater than value given. u -Haterial was analyzed for but not detected. The nurber is the Mininun Detection Limit. m])L ---NA -Not analyzed. \ 1/ -Tentative identification. 1 - ~/ -On NROC List of Priority Pollutants. II N.C. v;_v,u.,;_an 06 He.aLth Sv,.v;_c.u VHS 3068-0 {4/86 Labal!.a):a~y) \ I ( l ua/ 1 Hn/ka \ 1. • I • I ! , STATE LABORATORY Of PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. DEPAATMENT Of 11\JMl'N RESOURCES P.o·. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 21611 I I ORGANIC CHEMICAL ANALYSIS BASE/NEUTRAL ANO ACID I.AB NO l,fi)/ J•ii/ EXTRACT ABLES FiELD # aJNPOONO . TYPE ( J r \ r . ) ( ) UNITS ,r, , n I I)• • """"' .. n/ \ .. n/ka , ,,,; l 11<1/kQ uo/1 ua/ko nvrene /o/::i::io ' . - benzidine --'/,u:-o butyl benzvl phthalate J0/?=10 benzfalanthracene l chrvseoe . , 3.3-dichlorobenzidine 11'..<:'0 so1 bisf2--ethvlhexvl'nhthalate io/ '130 di--n--0etvr ohthalate 10/.J.:/o benzofblfluoranthene so7it.<ri benzo(klfluoranthene benzo(a)nvrene indeno( l 2 3-<d'nurene dibenzo(a.h)anthracene benzo(o h. il=rvlene "? . I : aniline <o,. .. I ' 11 ..... benzoic acid ! benzvl alcohol I 4--<:h loroani l i ne .. ,,, dibenzofuran '" /~,11 2--methyln•nhthalene ! 2--methvlohenol I 4--methvlohenol ' 1, : 2-nitroani 1 ine s-ot,t-<o 3--n i troan i l i ne i 4--n i troan i 1 i ne I 2.4 5-trichloroohenol ' ,., \ ' I I I I ' I I . I I I I ' I i ' I I i m:n1-l J -Estimated value. H ;z.'O/ SOI I.. K -Actual value is kllOWn to be less lhan value given. l -Actu.11 vdlue is known to be greater than value given. U -Material was analyzed for but not\detected. The nl.lTOer is the Minil1l..lTI Detection Limit. NA -Nol analyzed. I 1/ -Tentative identification. \ 21 -On NROC List of Priority Pollutants. -I N. C. D-i.v.u..-i.011 o 6 He.a.Uh SVI.v-i.c.ci VHS 3068-0 (4/86 LaboM..to11.y) \ I r J r l .. n/ 1 ""/ko un/1 ··"/ko 1 . . I -STATE LABORATORY Of PUBLIC HEALTH • · ' Laboratory No. DIVISION O~LTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES P.O. \BOX 28047 306 N._ WILMINGTON Sl, RALEIGH, N.C. 27611 __ ;?{'.! // 171,\ '. PURGEABLE COl1POUNDS ilate of Analysis --rlq/8,f i COl1POUND i µg/1 I COl1POUND Oichlorodifluoranethane !_ __ -·-· u --Chlorobenzene ------Chloranethane I ... -----·-· ~------·--Ethvlbenzene .tVinyl Chloride -..:L_ --~------ Brcm:methane I ----------·-1_ -·-----··-- -l. 1 l. 2-Tetrach loroethane _Q-Xylene ___ Chloroethane ·--m-Xylene ·------Tri ch lorofluoranethane I a-Xylene --··---· ✓1, 1--Dichloroethvlene I Styrene Hethvlene Chloride I Braooform -tert-Butvl Hethvl Ether I Isopropylbenzene -(Trans)l,2 Dichloroethylene I l, 1,2,2-Tetrachloroethane I Isopropyl ether 1 1-Dichloroethane I I -Braoobenzene n-P~vlbenzene . 2.2-DichlornnrfV'liane I -1,2,3-Trichloropropane (Cis) 1,2-Dichloroethylene I 2-Ch l oroto l uene Chloroform I 1,3,5-Trimethylbenzene . (BCH) Braoochloranethane I ' 4-Chlorotoluene ✓1 ;1, 1-Trichloroethane I pert) Butyl Benzene _ _1, 1-DichlorQQrooene --Pentachloroethane ✓carbon Tetrachloride -_L..?....!:-Trimethylbenzene -· ✓Benzene -------(Sec) Butyl Benzene -✓I 2-Dichloroethane ✓Tri ch loroethvlene !---·· 1,2-DichlorQQropane I ---·- p-Isopropyltoluene 1,3-Dichlorobenzene ✓l,4-Dichlorobenzene .. Brarodichloranethane I ' n-Butylbenzene DibNlTDll!thane I . 1.2-Dichlorobenzene Toluene I (8 isl 2 Chloroi<rnr=vl Ether 1 1.2-Trichloroethane I I ' 1.2 Dibraoo 3 Chlor~~ane -I I Tetrachloroethene -·--· ' ' l ,3-DichloroprQQane I -i . Dibrorrochloranethane I I -· 1,2,4-Trichlorobenzene Hexachlorobutaq[ene Nanhthalene --i I l , 2-Di broroethane (EDB) I -1-Chlorohexane I I/ ' -1,2,3-Trichlorobenze(!_'L__ -----I -·---·----·-----·-I --------· ·-----------------···---·-·· -··-! ------·-----·-·----·----------· . -· ·--. --· I I I \ HDL Hinimun Detection Limit for water (EPA Method 502.2), is 1.0 µg/1. I ' i J . Estimated value. I K .. Actual value is known to be less than value given. I. .. Actual value is known to be greater than value given. U -Material was analyzed for but notldetected. NA -Not analyzed. · \ l/ .. Tentative identification. \ ✓ .. Re~ulated voe I . Trthalanethane 1 1 N.C. Division of Health Services OHS 3068-0 (l/89 Laboratory) I ' I I I I II µg/1 / ---·-------- ··-·---·-· ·-· ·······--- -. .. . -------- ---- ··------· ------· ·----- ------- -· ----- -· --_ _l ____ I I ._I/ ---- - I '• . Nocth cLo~a.-Oepa.ctment of H"":e.n Res~ucc.Rfic···, f .. ,·v·. E. D. _·_··• J 01v1s1on of Hoe.1th Secv1ces : __ ,_.; ... . _· . . , Labocatocy Section · · ··• · · '• · P.i. Box 28047, Re.leigh, N.C. 27611: . ~ti#l!OO~-P/:;'p,o•: . . I . . . su~,liJBJ;qJ,.1.it~o·ii~CDH Env1conmontal Scionces Analysis Repoct 1'1fANtM •• '1 I I Name-of wn~Q_fi_~i:~t fJJ,,", ().J..._ ~ · ,1).,1. ,-:> oc Supply: ~Jf;jr~~' -/~;f,.A.'.:/, Addcess: , 1 • County: Ropoct to: Addcess:-"".[i;f;~~~~~~~~~--::::-;:;"7 ~~~~~~.46..ll.!L'l?, Oe.te _Collected By:~~Jt.&7I~~~~)l!....-.-,t.... __ Ane.lysis Oesiced:_:..,~U/.t.k~~;C,,-L..___ 6i\J ) A '• pr . ~ f) -e.~ , H-e , b ~( ,,1v_ o:rx-o. C'.Jv_d \ \ PHllOLEl:JM PROOtlCTS ) Le.boce.tocy Se.rople I Sample Descciption oc Reroe.cbl Results In Number-Nurobec I 9~11'75 I I I I I I I I I I . I I ' . ! I ' I I I J I I I I I I Date Date Received l/-:J ;;;> -3q /l;J '1£57 ' Extc-a.cted 5-1-MYl; P/1{. MW 8NA-5-..:l ~9 ,;116,Clll., 'fi,J OHS Fann 2364 Revised (1/87) Le.boce.tocy ' I I I I I I ~lJPERFU!\JD BRlU\JC!--1 /Jtii r'l,r-,.--, "". - . -~ "''"''--"'-H\l 11.UAU SfE ATTACHED SHEET($) Kildced A. Ke'rbaugh · Director 03V.tJl:)Jtj. eae1 8 J Yi\M H3MAA8 QMUlf!?iU2 • Human Resources rvica ·1 . I . . · \ • State .ratory of Public Holch SAMPLE A~AI:'.l'SES REQUEST P. o. Box 28047 I 306 N. Wilmington S::,ttr '.of Public Holrh P. 0. Box 2804 7 R.leigh .. 2761 I 'C"D Q<JS f58 52.?-\ FiddSamplcNumbcr_4-1-4.L..c..l~I-------------- ~~;::: ½~2-fi'L~~.:~:;12Rm. ~~ lilrnin.gton Strccr R.leigh, 27611 Co::=c.:::.u--a.tc I .:.:Ommen a. ';<ter (l) N'ater (2) ) __ Solid (5) i~IJb '.2-LtTel< __ Liquid (6) __ Sludge (7) __ Other (8) I I I INORGANIC CHEMISTRY :-act, b I es ,, Total I Results mg/1 --- - - Results mg/1 EE ATTACHED SHEET<S} MICROBIOLOGY :er 1 Colonics/JOOmls :-m Colonics/JOOmls Parameter I I Results mg/1 Parameter Results mg/1 __ Arsenic I __ silver __ Barium I __ Sulfates __ Cadmium ., __ Zinc I __ Chloride I __ Ph __ Chromium I __ Conductivity ,, __ Copper I _ms __ Fluoride i T0C ' -·---·· -·---__ lron I --_L=d I I --__ Manganese ! --I __ Mercury I --__ Nitrate I --__ Selenium I I -- ORGANIC1,CHEM1STRY Parameter _EDB · PCB's ~Petroleum ..X..Endrin ~~c, "D'le le! r"lf'- Results mg/1 I I . ----- \ ------I -::0.000/ I -"~==c.=.--<--- 1 1 __ Gross Alpha , __ Gross Bcca I Parameter Results mg/1 RADIOCHEMJSTRY Resulu PCi/ l , __ ---------------------! 1ults mg/1 :suits mg/1 1. I STATE LABORATORY Of PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES P.O. BOXl28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 I ' ORGANIC CHEMICAL ANALYSIS BASE/NEUTRAL AND ACID LAB NO I 0?11/ -,~ EXTRACTABLES FIELD it TYPE I I COl1POOND UNITS I /.,n/1 N-nitrosodimethvlamine Jl'\l2'fO bis (2-ch loroethvl )ether I 2-chlornnhenol '· ohenol ' 1 3-<lichlorobenzene ' I 1,4-dlchlorobenzene I 1.2-<lichlorobenzene I bis/2-chloroi llether I hexachloroethane I N-ni troso-<li -n lamine I ni trobenzene I ' i c:nnhorone I 2-nit~henol I 2. 4-<limethvlohenol I bis/2-chloroethoxvlmethane I 2.4-<lichloroohenol I 1 2 4-trichlorobenzene I n,mhtha 1 ene hexachlorobutadiene 4-chloro-<n-<:resol hexachlorocvcl,,,,.,ntadiene 2,4 6-trichlo~henol 2-chloron>nhthalene acen•nhthvlene dimethvl ohthalate 2 6-<linitrotoluene acen.:anhthene 2 4-<linitroohenol "0ll&.,:eo. 2.4-<linitrotoluene 11'1/.~'IO i 4-nitroohenol ,;-a°/,,_-ifo I fluorene /0/~30 I 4-chloroohenvlohenvlether ' diethvl ohthalate -·~ ' 4.6-<lini tro-o-cresol ..-o, 'if_,;, I diohenvlamine I azobenzene ,I, I 4-b=henvlohenvlether Ir,, '"30 I hexachlorobenzene ll'\/;r:i_r, I =ntachloroohenol so111.so 1 ohenanthrene Jr,/ :/'Ill I anthracene I dibutvl ohthalate I fl uoranthene \, I ,n1)L I J -Estimated value. H,.o/.S0/1.-\ -I l -- ' / ( ) ,on/ 1 .. n/ko K -Actual value is known to be less tha.n value given. ( l ,on/ 1 ,on/ko ( l .. n/1 .. n/ko ( ' .. n/1 ••n/kQ L -Actua] value is known to be greater than value given. U -Material was analyzed for but not detected. The nurt>er NA -Not analyzed. ! is the 11ininun Detection Limit. m'JJL --- 1/ -Tentative identification. I ~I -On NRDC List of Priority Pollutants.I N. C. V-<.v-<..-6-<.0n 06 Heal.th Se.Jtv-<.c.e/2 \ VHS 3068-0 (4/86 LaboJurto~y) \ ,I - ( l un/1 un/ko ' I I I • I STATE LABORATOOY Of PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUM.~ RESOJRCES r.o'! BOX 28047 -306 N. IIILMINGTON, ST., RALEIGH, N.C. 27611 I I ORGNHC mEMICAL ANALYSIS BASE/NEUTRAL ANO ACID LAB NO <./11//7.S- EXTRACT ABLES FIELD # O)Mf'OONO TYPE ( l ( l ( ) ( l UNITS {uo/1 m,t.1ro uo/ l un/kq HO/ I un/kn .. n/ I .. n/ko nvrene Jo/:i:i11 i,,L, benzidine I 'l"n1/1i60 butvl benzvl ohthalate /0f:;::,O benz(alanthracene 'I chrvsene . I, 3 3--<lichlorobenzidine .so-/it.. ,.,, bis(2-ethvlhexvllnhthalate /()/?30 di-n-octvI Dhthalate 'O/.s.::10 benzo(blfluoranthene so,-; benzolklfluoranthene benzo(alnvrene i ndeno ( l 2 3-<:dl nvrene dibenzo(a.h)anthracene benzo(a.h. il=rvlene .7 -I ! I ani 1 ine .--o /11,, er ; J - benzo1C acid ' I benzvl alcohol I 4-<:hloroaniline ~ ✓~ dibenzofuran IO 2-methvl n,mhtha lene ' ' 2-methvlohenol I 4-methvlohenol ,J ,' ' 2-nitroaniline s-ol,1 .. co 3-ni troani line ' 4-nitroaniline i 2 4.5 trichloroohenol ,, ,1 ' / I I I I ' ' I ' ' I ' ' I I ' I ' I I I m1H .. i J -Estimated value.· HiO/ Salt.. K -Actual value is known to be less:than value given. L -Actual value is known to be greater than value given. U -Katerial was analyzed for but not detected. The nunt>er is the Nininun Detection Limit. NA -Not analyzed. \ 1/ -Tent.a.live identification. ~I -On NROC List of Priority Pollutan,ts. N C V . . . . I • • -<.v.u-<.011 o 6 HeaUh Sviv-<.c.eJ.> VHS 3068-0 (4/86 Labo/t.a.to11.y) , I ( ) ( l .,,..,/ l 11n/ko .. n/1 Hn/kq '\ ' \ .STATE LABORATOHY Of PUBLIC HEALTH Q. Laboratory No. DIVISION OF HEALTH SERVICES N.C. DEPARTMENT Of HU11M RESOURCES. P.0.\BOX 28047 -306 N._ WILMINGTON Sl, RALEIGH, N.C. 27611 s/41- __ <lt)//'7'(: ___ PURGEABLE COl1POUNDS liate of Analysis . // ..i._'/__ 1 I - COl1POUND l µg/1 I COl1POUND Dichlorodifluoromethane I ~ ' -1··--· Chloranethane I -t------------------· ,'Vinyl Chloride ---- --Chlorobenzene ------- -Ethvlbenzene l l 1.2-Tetrachloroethane Brcmxnethane I ------------. -I------------1----e-Xylene -----------Chloroethane i Trichlorofluoranethane I ✓l. 1-Dichloroethvlene I m-Xylene a-Xylene . ----Stvrene Hethvlene Chloride I -Bromofonn tert Butvl Hethvl Ether I I !benzene ITransll 2-Dichloroethvlene I ' -1, 1,2,2-Tetrachloroethane lSQQr2QYl ether I Braoobenzene 1 1-Dichloroethane I n p~ .. Jbenzene 2.2 Dichloroor~ane l -I (Cis) 1,2-Dichloroethylene l,2,3-Trichlor2er2eane 2--Chlorotoluene Chlorofonn I (BCH) Branochloromethane ' ' 1,3,5-Trimethylbenzene 4--Chlorotol uene ✓1.1. 1-Trichloroethane I ITertl Butvl Benzene l 1-Dichlo ne I Pentachloroethane ✓Carbon Tetrachloride I ✓Benzene I , ✓1,2-Dichloroethane ✓Trichloroethvlene LK__ ___ : 1,2,4-Trimethylbenzene -·· (Sec) Butyl Benzene --e-ISQQr2Qyltoluene 1,3-Dichlorobenzene 1,2-DichlorQQr2eane ,, -·-· Bronodichloromethane -Dibronorethane {l,4-Dichlorobenzene -n-Butylbenzene 1 2-Dichlorobenzene Toluene I l, 1,2-Trichloroethane I . (Bisl 2 Chlorois l Ether 1.2-Dibromo-3 Chlo~~ane Tetrachloroethene I J.J. "'. ·-··-I I 3-Dichloroorooane I . [).. -Dibranoch loromethane r· -1,2,4-Trichlorobenzene Hexachlorobutadiene N•nhthalene ' 1,2 Dibranoethane (EDB) ' 12 3-Trichlorobenzene 1-Chlorohexane I ' I ·-· I .. -----.. ·-' ' ------------·----- . -------···-·-··•-···•-···-----·-------.L -·· ·-· I I I COlt!ENTS: I I I HOL .. Minirrun Detection Limit for water (EPA Method SD2.2), is 1.0 µg/1. I I J ·· Estimated value. , K •· Actual value is known to be less\than value given. I. .. Actual value is known to be greater than value given. U -Material was analyzed for but not detected. NA -Not analyzed. I 1/ •· Tentative identification. ✓ .. Re~ulated voe I . Tr1halanethane N.C. Division of Health Services OHS 3068--0 (1/89 Laboratory) µg/1 u.. -·--·--· -------- ·-·--- -· ... --· -· ----- ---·--· -··----I •••-· I-----i :.1 ·--= I I I -·· ! --i -i ·i;- - 'I I I I I I ·\ I North Carolina Department of Human Resources : Division of Health Services P,O. Box 2091 • Raleigh, North Carolina 27602-2091 I .J;:.;--:·12:-.; Cl .. i•·~;-ll"~i!1, l)GV/c:mr,i:' .·,· R. , .. 1:._' H. f.e11i1h:•:-M 0 .. , ?.'. 7 H.' David T. Flaherty, Secretary 1 State Health Director I I I I 1 17 April 1989 I I I Mr. Kelly Sheeks Environmental Health Supervisor Iredell Counj:y, Health Department P.O. Box 1268 735 Hartness Rd. Statesville,:Nc 28677 Courier 232 I • I I Dear Mr. Sheeks: I I SUBJECT: FCX -Statesville Oft'1-si te well sampling I As we discussed by phone, I ill\' supplying you '.vi th sampling cont'ainers to sample two off-site points near the FCX facility \in Statesville. At the public meeting on 5 April, two si,tes were identified that merit sampling. One is a well less than one mile south-southwest of the facility belonging to James Moore, 2102 Bristol Road, Statesville, NC (704) 872-4959. The other sampling point is a spring or rising stream.:to the northwest of the facility on land that borders the Burlington Industries plant. Both of these sites are valid sampling points for groundwater and both address citizen concerns. i I , I have arranged to have sent to you two organic sampling kits.\ Each kit consists of one box containing a styrofoam packer, ice packs, sampling containers, and a mailing label for return shipping to the State Laboratory of Public Health_l Each box contains 2 VOA bottles for volatile organics analy(ses and 1 2-liter bottle for extractable organics analy'ses. This should provide you with enough containers to \sample 2 sites for organics. I am also sending you a set of lab analyses requests sheets, partially filled out and\ labels to be attached to each lab sample container to identify the sample, partially filled out. I . ' ' I I I. Mr. Sheeks \ 4-17-89 ! page 2 1 I have! attached a brief review of sampling procedures for your information. If you have any questions about sample collection or filling out the sample analyses request Gheets pJ20~e ~~l}. m~ at f~~-9) 7_13--~80J ... I I GN/db/5.doc I I I I I I I I I I I ' ' ·1 ·1 I I I I I I I I I Sincerely, ~;;;; !::.isl, Ceologis, Superfund Branch Solid Waste Management Section DATE: TO: FROM: RE: ii i i i I I 10 Aprill 1989 I ' Lee Crosby I . I Grover Nicholson I I FCX-Statesville Public Meeting ' I On 5 April 1989 I attended a public meeting in Statesville, NC, concerning the FCX property there. The facility has been proposed for inclusion on the NP~ and presently US EPA is attempting to find and remove the buried pesticides. The meeting was held at the Monticello Fire Station. It began at 7 pm and ended about 9:30 pm. I have attached an agenda showing speakers present. I . . The meeting w~s orderly and most of the residents seemed well informed. I answere1d questions pertaining to the air and soil sampling conducted a'.round the site and about well sampling conducted and planned around the site. The residents expressed some concern about health problem~ associated with the pesticides. Surprisingly to. me, -however, was the: residents'question of whether or not removal of the buried wastes was the proper course of action. They requested that EPA allow theirjinput into any decision to remove the wastes and any decision on fina+ disposition of the wastes. EPA promised to consider their requests concerning final disposition, but removal was necessary and already underway. Don Rigger reported, however, that the wastes had not yet been located. I I i I I I i I I ' I ·1 I i I i I I I • UNl'fED STATES ENVIRONMENTAL PROTECTION AGENCY [ REGION IV I ! I I 31•5 COURTLAND STREET ATLANTA. Gl:ORGIA 30315 FCX SUPERFUND SITE STATESVILLE, NC APRIL 1989 INFORMATIONAL MEETING AGENDA. Introduction of Particioants ' . and Purpose of jMeeting I I &rergency ReSCXYl58 T551l8S ' I NPL 'RS!'rt,d i al Is'.sues I PUblic Health Iss11,;,s, I ?i1bli,:; Inv0lv,;,rrent I . . . . . . . . . . . . . .. .. . . . . . . H. Michael Henderson Community Relations USEPA -Region IV r:on Rigger on-scene Coordinator USEPA -Region IV Michael Townsend Remedial Project Manager USEPA -Region IV Chuck Pietrosewicz (ATSDR) PUblic Health Consultant Agency For Toxics And Substances Disease Registry H. Michael Henderson I QUESTIONS AND ANSWER SESSION ••••.••..•.•••••.••• All EPA & State Officials I I NJTE: Please hold all questions and canrrents until the end of the final presentation. I I Attorney Marcia ()wens of USEPA's Office of Regional Counsel and Grover Nicholson, a geola<Jist from the State of NOrth Carolina's Departrrent of Human Resources Superfund Branch• will, also, be available to answer questions during the questions and answer session. I MEDIA NOTE: All interviews of fJSEPA official should be cleared through the Comiunity Relations representative, Michael Henderson, before condlicting the interview. ·---fl I, (' !: ,, 1t I' ' t -. I •f .... I I I r -. • I ' . • !~:'b~b~p;rtmenr of Huffian Resources . Oivi~io:-i of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Health P_ 0. Box 28047 306 N. Wilmington Street Raleigh, 27611 I I Site Number Name of Site -'-N'--"C~D"---=-tJ___,9'--'b"'-_4-'-c'S-'---"13----'§~Z---'1 ___ Field Sample Number __ el_~-1---'2.~?~"1--------- FC, )(-:$ ,,9 r E:S VI L L E Site Location.--,-. _s~---',-;_-,q~r,~;s~:5---'v'_I~· =L~'--~E~~NC~~----- c _ ;1//CHOL,;;o,v \ ID# 3"1-Collected By 8 • t,(_/ I L '-I ,",-;Tl ';. Type of Sample: Environmental ___ Groundwater (I) ___ Surface Water (2) _K_ Soll (3) __ Other (4) Conceri.trate I __ :Solid (5) I __ [Liquid (6) __ Sludge (7) I __ Other (8) I Oare Collected Time --I 3~Z_I __ I INORGANIC CHEMISTRY Extractable• I Total . I . Parameter Results mg/ 1 : Parameter• Results ing/1 Parameter Results mg/ l __ .Arsenic I __ Arsenic· __ Silver __ Barium I __ Barium __ Sulfates __ Cadmium I __ Cadmium· __ Zinc _._Chromium I __ Chloride -Ph __ Lead. I __ Chromium . -. _. Conductivity __ Mercury I __ Copper _TDS __ Selenium I __ Fluoride _· __ TOC I __ Silver I __ Iron -- I _· _Lead ----I _·_ Mang~nese ---- --I __ · Mercury --,. --. I __ Nitrate . -- ! __ Selenium ' ---- I ORGANIC CHEMISTRY Pilrameter _P&T:GC/MS __ Acid:B/N Ext- _ TOX Parameter Results mg/ l Parameter _·. _EOB _·_PCB's --------'' __ Petroleum _x_Endrin iundane .~td..r---.""" MICROBIOLOGY ' i __ (MF) Coliform Colonies/lOOmls I __ (MPN) Coliform Colonies/lOOmls I I --' -- I Reported By DHS 3191 (R~·vi 7/85) Solid :ind Ha::irdous \X/astc ( Review 7 /87) Results mg/ l Parameter _L Methoxychlor _L Toxaphene ~2.4-0 L 2,4,5-TP (silvex) ~:L?~~'Pf,?!'.!~l __j5,_ P12 T t,..l.,rda"e. RADIOCHEMISTRY Results mg/ 1· ~g;,~~ <. O.i ~/L <0,/0 --=:- Parameter Results PCi/ 1 __ Gross Alpha __ Gross Beta -- -- Date RepOrl,!.cl ·:z -_3-6° L res-r. 9 o-a tllrb Dare Analyzed ;;,...--" I -VP &,:·oll)fB-"(l,....,_,) ___ _ Lab Number 1 oa3; / ., I I · N. C. b'cP3.rcmcnt of Hunlan Resources . Divi~ion of Health Services 1• . ! 5';'.°'MPLE ANALYSES REQUEST • St:ltc Laboratory of Public Heald, P. 0. Box 2804 7 306 N. Wilmington Street Ralci~h, 27611 Site Number . I __ N~C~D~~t)_'J~b~_4-~5~$~~-Z~:j~--Field Sample Number _4-~Z~r_V ___________ _ Name of Site __ F;~C=X'--_~:5~-r~'9~T~E~S~1'1'-;l~1~L=L~E~-----Site )..oca,ion,_ _:5,,q TE:5v'/ LLE Collected By ~C_. _,V,~l~C=M=O~'-=,;=r9~AJ~--ID# ~3~°'1-___ Date Collected ~-'---'C,. 8 • t,(/ I I-'-I ,rr'fl S. Type of Sample: Environmental ___ Groundwater (!) ___ Surface Water (2) _L Soil (3) __ Other (4) Extractables I Concent,;ate __ S~lid (5) __ Liquid (6) I __ Sludge (7) __ Other (8) I :'>,4/Y/ PL£ INORGANIC CHEMISTRY I Parameter Results mg/ 1 I ' Parameter Results mg/ 1 ·_·_· Arsenic j• _. _Arsenic __ Barium I __ Barium __ Cadmium __ Cadmium _._Chromium ! __ Chloride __ Lead ! __ Chromium __ .Mercury ' __ .Copper __ Selenium i __ Fluoride I -__ Silver __ Iron --__ Lead --I __ Manganese --I __ Mercury· --_._ Nitrate . --I __ Selenium ' ' ORGANIC CHEMISTRY 4~/1.fANAG~l' Total . •_ Parameter _·_silver. __ Sulfates __ . Zinc _Ph -. _.Conductivity. _ms _TOC -- -- ---- -- -- NC Results mg/ 1 P3.rameter Results mg/1 Parameter _Results mg/1 . Parameter Results mg/1 _P&T:GC/MS __ Acid:B/N Ext. _TOX _EDB __ PCB's __ Petroleum ~Endrin ______ --------;i ·-1LLindane I l',. I,!~,~ MICROBIOLOGY ' Parameter I __ (MF) Coliform Colonies/J00mls I __ (MPN) Coliform Colonies/!O0mls -- I --I DatcReceiv~~t,--79 v1{x Date Extracted 7 f'1VP ll.,::P-ffi PW Reported Oy DHS 3191 (R,:viscd 7/85) Solid :"Ind Ha:ardous \Vastc (Review 7187) ~ Methoxychlo; _:f.__ T oxaphene --~~:2~~~pjiij~~_i.__ 2,4-D _i._ 2,4,5-TP (silvex) -::::::~-'-':'a.-,W,=-i_x_ :Di?I. lk Cl,.( b RADIOCHEMISTRY Parameter R~sults PCi/ 1 __ Gross Alpha __ Gross Beta -- --. Date Reported jf-p€.S7, . .µQ/1 Date Analyzed ,;;J.:'f-fr/1/p 3-80-'iWPu) Lab Number SOOJOO · J:i. C. ciejJJ.rtment of Huffian Resources . Divi'iion of Health Services I i. . I SAMPLE ANALYSES REQUEST I • State Laboratory of Public Health P. 0. Box 28047 306 N. Wilmington Street Raleigh, Z 7611 I Sire Number __ N~C~D~~tJ~'l~6~_+~5~'o~!>_Z~-1 ___ Field Sample Number _ _:f_Z=-:fc_:__/ __________ _ Name of Site _c_h_,C,.,_.,)(,__-__.:$"'-'-r-'/1-'-'T_E=:S=v-' 1 l~L,,,_,L"-"E:"-------Site Location, ..5 ,,-,, TE$ II' I L.-LE Collected By _C_. _A/._1~c~1-1=o~L~.;~<9_N __ ~ ID# ~3,,,_"'1-"----Date Collected -:--:i'---'--:-"''-"'::;;;;;;_;~;,;;=- 8 -t{/1,t..L-1,q-;1'1$ Type of Sample: Environmental ___ Groundwater ( 1) ___ Surface Water (2) _)(._ Soil (3) __ Other (4) Concent~te __ S~lid (5) __ Liquid (6) I _·_ Sludge (7) __ Other (8) I NC Time /31-'if _5,q,n PL€ INORGANIC CHEMISTRY Extractable• Parameter _._·Arsenic __ Barium __ Cadmium _··_Chromium __ Lead __ Mercury _·_ selenium __ Silver Results mg/1 Parameter• ------~' __ Arsenic __ Barium __ Cadmium· __ Chloride ------~' __ Chromium· __ Copper __ Fluoride . __ Iron __ Lead ______ -------~' __ Manganese -.-Mercury.· __ Nitr~te ·. __ Selenium Results mg/ 1 Total Parameter· __ Silver __ sulfates __ Zinc _Ph __ Conductivity .. _._ms··· · _TOC Results mg/1 - ORGANlC CHEMISTRY P3.rameter _P&T:GC/MS __ Acid:B/N Ext. _TOX Results mg/1 MICROBIOLOGY Parameter. ! __ (MF) Coliform Colonies/ IO0mls __ (MPN) Coliform Colonies/lOOmls Parameter _EDB __ PCB's __ PetroleuITl _LEndrin ·....!::_undane )(. 1 C, k! ,-, " Results mg/ l Parameter _:L_ Methoxychlor · ~ Toxaphe~e. · _L2,4-D · -=::::.!!.l!_..L!,!..J~ffi...j....!::_ 2, 4 ,5-TP ( silvex) =J.l..!.L!,!._/;,.'R£.~_L DI? T Results ;..g/ 1 I. [b,._d_ ~ ~ RADIOCHEMISTRY Parameter _._·_·Gross Alpha __ Gross Beta Resuits PCi/ i Date Reponed • . P6Jl_· Q oa --i-1:iuJi- Dare Analyzed -t -" I -VP .;i.-a0-$?.f4) Reported By --------~~-------Lab Number ---~~~.J'_!)c_·' _Q_3_· ~(_)cc1c._ _______ _ DHS 3191 (Rc:-vised 7/85) Solid :ind Ha~:irdous Waste (Review 7187) N. C'. l)...-f~artment of Hum.an Resources · Div,ision of Health Services I tMPLE ANALYSES REQUEST • State Laboratory of Public Health P. 0. Box 28047 306 N. \X-'ilmington Street Raleigh, 27611 Site Number --'-N-'----"C'-'D""------"'cJ_,9,...,::."'-_4-'-----"Sc....,,'S~5=--=Z:..:l ___ Field Sample Number _4-.,_,Z.c:..1.,__,7-::.._ _________ _ Name of Site _ _.c_F,_,.C,=)(_-_2:;;;"--'--,--',9.:....:r---=E~:S=v''--'1'--=L"-.=L'-'=E=--------Site )..oca,ioq-_:5,-,q TE!,V/ LLE NC Collected By =C'-_'--',<l.--'-1-"c'--'J-t-'--"o-"L-'--',;;,,_o=--cN-=---'--ID# __,3"'--'"1-'----Da tc Collected 5 FE is 'o 9 . Time I/{) z___ 8 • I-{/ I ~ ,_ I ,rr1'1 S. i Type of Sample: ' Environmental ___ Groundwater (I) ___ Surface Water ( 2) ~ Soil (3) __ Other (4) I Concer;itrate. __ 1 Solid (5) __ [Liquid (6) __ !Sludge (7) __ '.Other (8) I /4 AIJ><:-1.AJ INORGANIC CHEMISTRY Extractable• Parameter __ .Arsenic __ Baritim __ Cadmium· _._ Chromium_ __ Lead __ Mercury __ Selenium __ Silver P.lramei:er Results mg/ 1 : ·, Results mg/ 1 Parameter __ Arsenic __ ·Barium __ Cadmium_ __ Chloride __Chromium __ Copper __ Fluoride _ __ Iron __ Lead __ · Manganese __ Mercury --Nitrate. __ Selenium Total Results mg/ 1 · _ . Parameter _·_silve~ ___ Sulfates ------~--__ Zinc _-_. Ph· __ ._Conductivity _--_TDS ····· _TOC _ ORGANIC CHEMISTRY Parameter Results mg/ 1 Parameter __ P&T:GC/MS -----~• __ EDB _______ L M~thoxychlor __ Acid: BIN Ext. _-_ PCB'.s -___L Toxaphene - __ TOX ------+' __ Petroleum -----,-,=---1-Z,4-D _____ ------~! 1-Endrin <"'' /0 ·· '/< 2,4,5-TP (silvex) _____ -----'----'-i ~Lindane * <r"·a,/O'· ----_::L._ DDT ; ~D,clJ.--,,-,. ~"'-10' ~ 'f.. ri.,(o.....l~,..., MICROBIOLOGY !lo>:'K -rR.ACE /t7YJ61U./r .JJeT~!o,(!{, RADIOCHEMISTRY ' . ' Results mg/ 1 Results mg/1 ~~: ~% -,:o. I m-J IL ..:o.l ·--"-IL <:,,.,, , IO ~ -I. .• A -~--::_,·_ I,' Parameter I Parameter'• R.;sults PCiil __ (MF) Coliform Colonies/lOOmls I __ (MPN) Coliform Colonies/lOOmls I __ Gross Alpha _-_Gross Beta · Date Received ;;J..-{,-5i'q \if', AA' -Date Reported -f>csr _ -~Q),h-ff>es7. a Date Extracted 2--7-%11 VP i~,1~9 ew DatcAnalyzed ,;J..--, -Y1-VP _________ _,_ 1 ________ Lab Number . ~00302 Reported By DHS 319 ! ( Rl·viseJ 7/85) SllliJ :rnJ Ha::irdous Waste (Review 7 /87) N. c: Oa,iactment of Human Resoucccs · Oiv,ision of Health Services I : tMPLE ANALYSES REQUEST • State Laboratory of Public H~:ilth P. 0. Box 28047 306 N. Wilmington Street Raleigh, 27611 I Site Number __ N~C~D~-t>~'i~~~-4~5"~'o~£~Z_-1~---Field Sample Number __ 4-~Z-~7-~3~----------- Namc of Site __ F,~C,=)(~--=~~'~19~T~E~:S~-~ll'~I ~l~L~L~G~-----Site Locaiio'!-_ _:5-,,q TE:5 V' / LLE I Collected By ~C~-_ftl'.~1~C~M~O~L.~,;~r9~N ___ ID# ---'3=----;z.'-------Date Collected ~.2...---:-=£..£..---.~ 13. ;,u,,_,_,,q--;11s. Type of Sample: Environmental ___ Groundwater (I) ___ Surface Water (2) __ i.._ Soil (3) __ Other (4) ' Concent'rate I _-__ Solid (5) __ l.:iquid (6) ' __ Sludge (7) __ Ocher (8) .5AMPL£ BBT INORGANIC CHEMISTRY Extractables I Total Parameter Resultsmg/1 I Parameter• Results mg/ 1 Parameter I -- __ .Arsenic ' __ Arsenic __ -Silver.· ., --Barium _-_Barium __ Sulfates __ Cadmium I __ Cadmium: --_-_Zinc· _._Chromium __ Chloride _-_Ph· ' __ Lead __ Chromium __ . Conductivity __ _· _Mercury I __ Copper _-_TDS. - - ,· __ Selenium __ Fluoride _TOC : , __ Silver __ Iron -- i __ Lead ----' ___ Manganese ---- --i __ Mercury -- --: __ Nitrate -- --__ Selenium -- I ORGANIC CHEMISTRY P3.rameter Results mg/1 I Parameter Results mg/ 1 Parameter _P&T:GC/MS I _EDB _:i._ Methoxychlor __ Acid:B/N Ext. __ PCB's _LT oxaph~ne _TOX __ Petroleum. ...:L.. 2,4-D I _1_Endrin <:LJ. I rJ --.-L • )t 2,4,5-TP (silvcx) . 7'--<:O, • '/. Dl>T Results mg/ 1 : . . C Results mg/ 1 . <al L0_/2/).m <(), ,,;1-0 DP,ro... ,: o. l_ .,:;1 l I, - (O.I m,gU-.,...,...,_IO-~-· -·=:pcJ} X o.l!:f tnj (Li __ -Lindane _ )< "T>"'j .... I L._I-. ~o, 10 . J( "'"" ,---,J a,.('.ljl! . <,.,, ., --,,,,,.~ MICROBIOLOGY , I . . . T RADIOCHEMISTR ~ :,.-1,v,Cti.Arn<><JNT ~.i; P~rameter I __ (MF) Coliform Colonies/lO0mls __ (MPN) Coliform Colonies/lOOmls I I --' --I Date Received 2---b -79 JI~!§,_ p€sr - Date Extracted ,;z.. -7-?'1 VP -a"l'7-8"! ew Parameter Results PCi/ 1 0 ,0 'f-'P __ Gross Alpha __ Gross Beta -- -- Date Reported -P~- Date Analyzed ~ -/0 -:f'-/ Vf> 1-J.o,J.)-' a-ao-!f) P4.> Reported By ---------------Lab Number. -~9~()'--'-· ,_,Q,._~=-1--'0_J:::._ ________ _ DH$ 3 I 91 ( R<:vised 7185) Solid ;md H~zardous Waste ( Review 7 /87) n N. C. · DeP3.rrment of Human Resources Division of Health Services I. . • , SAMPLE ANALYSES REQUEST State Laboratory of Public Health P. 0. Box 28047 306 N. \Vilmington Street Raleigh, 2761 \ I Site Number Collected By l3 . Kl I '-I-, ,rrTl s. Type of Sample: Environmental ___ Groundwater (I) ___ Surface Water (2) __ Soil (3) _L Other (4) Concentrate ' __ Solid (S) I __ Liquid (6) I __ Sludge (7) I __ qther (8) Date Collected 3' FEB 'o'CJ Time t#Z:-/ /l'JZ.<- ll8 /l?/L.l.~ £ • -~!' • ~~ I INORGANIC CHEMISTRY ~~~ ., .~~ ' Extractable• ' Total -~ Parameter Results mg/ 1 Parameter Results mg/ 1 -Parameter Results mg/ 1 ., __ .Arsenic I __ · Arsenic __ · Silver .. ' __ Barium I __ Barium __ Sulfates __ Cadmium .. •} _·_cadmium __ Zinc ' _·_ Chromium __ Chloride _Ph __ Lead I _·_. Chromium . __ . · Conductivity ·, __ Mercury I __ . Copper _· _ms __ Selenium I __ Fluoride _Toe __ Silver _·_Iron --I __ Lead ---- --_·_ Manganese -- --__ · Me!cury -- I __ Nitrate. . ---- --__ Selenium -- ' ' ORGANIC CHEMISTRY Paraineter Results mg/1 . Parameter _EDB _P&T:GC/MS _· _ Acid:B/N Ext. _TOX -~-----' __ PCB'.s __ Petroleum __x._Endrin -~-Lindane )( .r\ MICROBIOLOGY Parameter __ (MF) Coliform Colonies/lOOmls · ' __ (MPN) Coliform Colonies/lOOmls I ' -- --I Date Received ,;;..-t, -n VP, A A-I_ ~es-r-) Date Extracted ,9-6 -'i{'f VP Reported Oy DHS 3191 (Revis..:J 7185) Solid :rnd Ha:ardous \X/aste (Review 7 /87) Results n Parameter Methoxychlor · T oxaphene . .:<="::,.2',.L::.:IJLC.=='F-; 2,4-D -</ 2 4,5-TP (silvcx) r ...:-<"~Sc 1-o <:: RADIOCHEMISTRY Parameter R.:sults PCi/ 1 _·_ Gross Alpha __ Gross Beta -- -- Date Reported-----~------------- Date Analyzed ~ -[f-?'J VP Lab Number .N. c: D~Partment of H~man Resources Oivi.sion of Health Services • ! SAMPLE ANALYSES REQUEST • State Laboratory of Public Health P. 0. Box 2804 7 306 N. \Vilmington Stri:et Raleigh.27611 I __ N~C~D~~cJ~'l~b~_4~5-·:-"$_5_l~i ___ Field Sample Number __ f~2--_1-_5 __ · _________ _ I Site Number Name of Site __ F.~C,~X'~--:;5=~'~,9~T_E=:5,~v'~1~'-~l-~£ ______ Site Location,. .:5 ,,q r~-S VI l-'-E NC Collected By _c_. _,v,_,~C~h=O~'-~,;;~o_N ___ ID# ~:3~-;r. ___ Date Collected ~-5'-....,_F.__,,,Ec..::B'-_'S',,_9,____ Time _tf:i'.:'771~·:=::,.~_ 8. J,(/1 Ll-1,',-"1$. Type of Sample: Environmental ___ Groundwater (1) ___ Surface Water (2) __ Soil (3) L_ Other ( 4) Concentrate __ Solid (5) i __ Liquid (6) __ Sludge (7) __ Other (8) ! -✓ou_· N INORGANIC CHEMISTRY Extractable& Parameter __ .Arsenic __ .Baiium __ Cadmium· _._Chromium __ · Lead __ Mercury __ Selen.iuin · __ Silver Result& mg/ 1 Parameter• __ Arsenic __ ·Barium __ ·Cadmium __ Chloride __ · ChrOmiU:m ------~. __ Copper _______ 1 __ Fluoride. __ Iron __ Lead __ Manganese __ Mercury __ Nitrate. ______ ----------;' __ Selenium Results mg/ 1 .. -: Paraffie~er __ Silver _· -Sulfates · __ ZinC _·_Ph -. __ Conductivity _ms _TOC Results mg/ 1 ORGANIC CHEMISTRY P3.rameter Results mg/ 1 Parameter _EDB _P&T:GC/MS __ Acid:B/N Ext. _TOX ------~' __ PCBls __ Petroleum ~ Endrin ___L_l.indane MICROBIOLOGY Parame.ter I __ (MF) Coliform Colonies/lO0mls I __ (MPN) Coliform Colonies/lOOmls I ' -- --I I Date Received t?--6-79 VF; 611 . f'l!:'ST° I Date Extracted ,;i-6-f"'IVP Reported By OHS 3191 (Rc:-vised 7/85) Sulid and Ha;ardous Waste (Review 7187) >< el ,n Paramet~r __ Gross Alpha __ Gross Beta -- -- Parameter Methoxychlor Toxaphene 2,4-0-. 2,4,5-TP (silvex RADIOCHEMISTRY Results PCi/ 1 Date Reported·=,,.,-------------~----~sT Date Analy:ed ,)._-'r-"6Cf1/p Lab Number qQQ~'.05 .N. c'. D~i1artmenc of Human Resources Divi.sion of Health Services !MPLE ANALYSES REQUEST • · State Laboratory of Public Health P. 0. Box Z&).;7 306 N. \Vilmington Str<!er Raleigh, 2 76 l l Sire Number NCD· cJ'tb--1-S!'o £27 Field Sample Number __ 4~Z~'rb _____________ _ Name of Site FC)(-:$,/9TE;SV'I LL£ Site Loca;ion_.. ..:5 r,q TES v' It.LE NC Collected By C. l.l1c1-10L~ON .ID# 3-;t-Date Collected 5 FEE 'f{'"J Time I04D B . Kl I ,_ I-I ,q-,n > T ypc of Sample: Environmental Concentrate C ns ___ Groundwater (I) ___ Surface Water (2) __ Soil (3) _._ Solid (5) :5Afr1PLE A/4:, CVLh72=--='-'--'-=-'-..c.....c=~-'--=..c.,;".,;f _'/-._ Other ( 4) I __ Liquid (6) _·_ Sludge (7) ' __ Ocher (8) I INORGANIC CHEMISTRY Extraetables Parameter __ .Arsenic _·_Barium __ Cadmium _._Chromium __ Lead __ Mercury __ •Selenium __ Silver -- -- -- -- -- Pclrameter _P&T:GC/MS __ Acid:B/N Ext. _TOX Results mg/1 Results mg/ 1 i I I ·i". I I ; ; . I I I I MICROBIOLOGY Parameter I __ (MF) Coliform Colonies/lO0mls I __ (MPN) Coliform Colonies/lOOmls I -- --I Date Reccivecl $-6 -?'J VP, if/{. p .:, Date Extracted ,,;i.-{, -'fr"[ i/P Reported By DHS 3191 (R,.-vis..:d 7/85) S\1\id ;rnJ 1--1.a:ardous Waste (Re\'iew 7 /87) Total ~M~til'\G~· -Parameter• · Results mg/l .·. Parameter Results mg/ 1 __ Arsenic __ Silver -·-Barium __ · sulfates _._·_Cadmium __ Zinc __ Chloride _·Ph _._. Chromillm ·. · __ . eonducnvitv __ Copper _·_ms··· · . __ Fluoride _TOC - __ Iron -- __ Lead -- __ Manganese .. __ Mercury· -- _·_Nitrate. -- __ Selenium -- ORGANIC CHEMISTRY Parameter _EOB _·_PCB:s __ Petroleum _l:_ Endrin ·_LLindane :>< I> ,c,:.ILr-~ I' . Parameter _L Methoxychlor ------~· L Toxaphene . _c__2,4-D _;::'=-!-~~LL"""'"f'lf.2__ 2,4,5-TP (silvex) --=-~~~~=-1..L.. PDT < I. lo r<!. ane -=:: RADIOCHEMISTRY Parameter Results PCi/ 1 __ Gross Alpha __ Gross Beta -- -- . Dare Reported ;a.a...,--~·-~-------------P&S'T Date Analyzed ;9..-'8'-'i'f ·J/p 000-:ioc Lab Number t..1"-~· ~.-. 'U .N. C. oepartment of Human Resources Division of Health Services ·!· . • j SAMPLE ANALYSES REQUEST Smte L,boratory of Public Hcalch P. 0. Box 28047 306 N. \Vilmington Street Raleigh, 27611 Sit!! Number __ N~C~D-~cJ_9~b_4--'-'STC.,1~S~~~l~-1~--Field Sample Number -~'r~Z~T_-=1-__________ _ NamcofSite FC,)(-:$r/9TE:Sll'ILL..£ CollectedBy C. ,il1c1-tol-,;;.o,v ID# 3-;z 13-1-{/,,._,...,,q-,.,,s. Type of Sample: Environmental ___ .Groundwater (1) ___ Surface Water (2) __ Soil (3) _L Other (4) Concentrate ' __ Solid (5) __ i:_iquid (6) _·_ Sludge (7) I __ Other (8) Site Locaiion_. _:5,-,q TESV/ LLE l\(C I INORGANIC CHEMISTRY Extractables Total 1-8 Parameter Results mg/ 1 Parameter• Results mg/ 1 · · ParametCr Results mg/ 1 __ .Arsenic __ Barium __ cadmium. _._Chromium __ Lead __ Mercury __ Selenium. __ Silver __ Arsenic __ Barium ------~I __ Cadmium ______ .c.l ____Chloride -------'~ __ Chromium· __ Copper• __ Fluoride . __ Iron __ Lead -~-----~-----~i~· __ Manganese ------~' · ___ M.ercury __ Nitrate· _ __ Selenium ·_· _Silver __ Sulfates __ Zinc· _·._Ph -•_.Conductivity _ms·· _· TOC ORGANIC CHEMISTRY P.i.rameter Results mg/ 1 Parameter _P&T:GC/MS __ Acid:B/N Ext. _TOX ------~' __ EDB MICROBIOLOGY Parameter ' __ · (MF) Coliform Colonies/lO0mls j __ (MPN) Coliform Colonies/lOOmls ' I -- I -- ' I DateReceive~~~-?9 VJ;,A~ Date Extracte~ ;2-t(;, 'i?1z VP __ PCB's __ Petroleum IC Endrin ·T-undane Results_ . Parameter __ . Gross Alpha __ Gross Beta -- -- · P.irametet'· . Methoxychlor .. . Toxaphene 2,4-D 2,4,5-TP (silvex R.;sults PCi/ 1 Date Reporter-lu.-,,r,,..,,,..---~-------------Pl:i:S7 . . Date Analyzed ;il.--: f-8'Jyp Reported Dy -----------'---------Lab Number DHS 3191 (Revised 7/85) Solid and Haz:Hdous Waste (Revkw 7 /87) _N. C. oe~1artment of Hum.an Resources Division of Health Services tMPLE ANALYSES REQUEST • St:i.tt: Laboratory of Public H~alth P. 0. Box 28047 306 N. \'Vilmington Street Raleigh, 27611 Site Number __ N~C~D~~tJ~9~b~_4~S-;-' ~'i)~f>~Z.~-1 ___ Field Sample Number __ f~Z...~7-~""if~---------- Namc of Site __ F.~C~Y~--=:$~r~"'~r~E~:5~'t/'~t_L~l.~£~-----Site Location_.. .5 ,,q TE:5 V/ Collected By ~c_. _Al.~'~C~l-t=O~L=;;;~o~N ___ lD# _3~~---Date Collected -'"'---'---""--:afi'. 13. H./, ,._,_, ~r11S. Type of Samole: i Environmental ___ Groundwater (I) ___ Surface Water (2) __ Soil (3) _f-._ Other ( 4) I Concentrate ' __ Solid (5) I __ \.,iquid (6) __ Sludge (7) I __ Other (8) :5;9,nPL£ 1.2 ,4-,,J I<:. I A.J INORGANIC CHEMISTRY Extractable• I Parameter Results mg/ 1 ' Parameter Results. mg/1 __ -Arsenic ' __ Arsenic . __ Barium I _· _Barium __ Cadmium . ' __ Cadmium· __ Chromium ! _._Chloride __ Lead .•, __ Chromium __ Mercury I _·_-Copper _._Selenium i __ Fluoride __ silver I __ Iron --I __ Lead --_·_Manganese ! __ Mercury --I __ Nitrate_ -- --I __ Selenium I ORGANIC CHEMISTRY P.i.rameter Results mg/ 1 Parameter ------~' __ EDB _______ , __ PCWs _P&T:GC/MS __ Acid:B/N Ext. _TOX __ Petroleum 1-Endrin ______________ ·, LLindane )<. d MICROBIOLOG~ Results Total . • · ParamCter __ Silver __ sulfates __ Zinc _Ph __ ··.Conductivity_. _·-_IDS... . _Toe -- -- --.. -- -- -- Par.imeter·· -L-Methox.ychlor . L Toxaphene · L2,4-D . 2 4,5-TP (silvcx) L ut-7F Results mg/ 1 Parameter I Parameter R.;sults PCi/ l __ (MF) Coliform· Colonies/lOOmls __ (MPN) Coliform Colonies/lOOmls ' -- -- ' Date Received ,;;z .,.. t -21 VP. /)i} ,Pfi!:sT_ J : Date Extracted .:Z. -&, -8':f VP 1 I Reported By DHS 3191 (R,:visd 7/85) s~llid ar,J Ha:ardous Waste (Review 7 /87) __ Gross Alpha __ Gross Beta . -- -- Date Report~ _ • Oare Analyzed~ 8'.:-"f9YP Lab Number 900308 N. C. Department of Human Resources Divis-:On of Health Services • j SAMPLE ANALYSES REQUEST • I Site Number Name: of Site State Laboratory of Public Health P. 0. Box 2804 7 306 N. Wilmington Screet Raleigh, 2 7611 --'-N-'--"C"--"'D--=tJ'-'t,_b""---_4-'---'5'~:S'-'£'----'Z'--1'----Field Sample Number _ ___,f_,l,_'t,_9 __________ _ I FC,)(-:£,,;<>rE:s,), LL£ Collecred By 8. /U I '-L-I ,9-;1'1 > ~~~~m~: j Environmental Concentrate ___ Groundwater (I) ___ Surface Water (2) __ Soil (3) ~ Other ( 4) I . __ Solid (5) I __ L,iquid (6) ' _·_ S,ludge (7) __ Other (8) I RA-#01<:11,J INORGANIC CHEMISTRY Extractahles Parameter __ Arsenic __ Barium __ .Cadmium _._Chromium __ Lead _·_Mercury __ Selenium __ Silver -- -- -- -- -- Pilrameter _P&T:GC/MS __ Acid:B/N Ext. _TOX Results mg/ l Results mg/ l ' i ' i ! I I I I . I ' : I ,I Parameter Results mg/ l __ Arsenic __ Barium __ Cadmium __ Chloride __ . Chromium· __ Copper __ Fluoride __ Iron _Lead __ Manganese __ MercurY __ Nitrate __ Selenium ORGANIC CHEMISTRY Parameter _·EDB __ pews __ Petroleum LEndrin Resul ______ -------~• _L_Lindane "l MICROBIOLOGY Total Parameter __ Silver __ Sulfates __ Zinc _Ph· __ . Conductivity _·_ms _·_TOC -- -- -- -- -- -- Parameter _)!,_ Methoxychlor L.. Toxaphene 2,4-D 2,4,5-TP (silve RADIOCHEMISTRY /-C, Results mg/ l Parameter .J Parameter Re.suits PCi/ l _·_(MF) Coliform Colonies/lOOmls I __ Gross Alpha __ (MPN) Coliform Colonies/!O0mls I __ Gross Beta ----i ---- I Date Rccciv~~f}-7q VP_, 1111-; Date Exrracwl .2: -6 -';/'1 VP Reported By Date Reported . Date Analyzedf";J!-9-5JCJYP ---------~-------Lab Number 900309 DHS 3191 (Rt.•viscd 7185) Solid and Hazardous \Vastc (Review 7187) · N~ ·C. Department of Human Resources Division of Health Services 1 I.MPLE ANALYSES REQUEST. State Laboratory of Public Health P. 0. Box 28047 306 N. Wilmington Street Raleigh, 27611 Site Number _ _.:_N-"-'C"--"D::....__,C)"'--'-'j~b"-_4:._·_.,,S-'--' _,S::...._!>==---.:Z::.-1.:.._ ___ Field Sample Number _1-_,___-Z.-'=-...,'J'---D-=--------------- Name of Site _.:._F._,.C,=)(--_~~=--1--'/9-'----'T'-"E'-'S""--'~'---''-----'L=--..eL'---"£=--------Site J.,ocaiio~---=__5'-=--,;'-'--,q--'----r,'---"c,S'-"'---'I.I''--'/'---. .=Lc:cL=cE=a... _ _,__NC--"----""------- Collected By -=Cc....:... _Al.:..__,t_,C"H'--'-"O'--'L=,;'-"<9'---'-'N=---.....:.-ID# __,3=--;t-'----Date Collected 5 FEB 'S'"l Time I I l 5'" 8 . t{_/, L L-. / ,q---r1'J $. Type of Sample: - Environmental ___ Groundwater (1) ___ Surface Water (2) __ Soil (3) _x__ Other (4) Concentrate I __ Solid (5) ' __ Liquid (6) __ Sludge (7) I __ Other (8) l3B'T INORGANIC CHEMISTR Extractables Parameter __ .Arsenic __ Barium __ Cadmium _._Chromium __ Lead __ Mercury __ Selenium __ Silver Results mg/ 1 Parameter. __ Arsenic __ Barium __ Cadmium· __ Chloride __ Chromium· __ Copper __ Fluoride __ Iron __ Lead __ Manganese __ Mercury· __ Nitrate __ Selenium Results mg/1 ORGANIC CHEMISTRY P3.rameter Results mg/ 1 Parameter _P&T:GC/MS __ Acid:B/N Ext. _TOX MICROBIOLOGY ' Parameter I __ (MF) Coliform Colonies/lOOmls ! __ (MPN) Coliform Colonies/lOOmls ' --I --I _EDB __ PCB's __ Petroleum L Endrin LLindane Parameter __ Gross Alpha __ Gross Beta -- -- Parameter __ Silver __ Sulfates __ Zinc _Ph· __ Conductivity _ms··- _Toc Parameter RADIOCHEMISTRY Results mg/ 1 Results PCi/1 Date Receive~/-:(,, -';?C/ t/~ Date Extracted ,z:-/;, f"f VP Date Reporr~ ... ~---~------------- Datc Analyzed Jt -Y-f9-f/p Reported Ily ----------~--------Lab Number ono ,;-1: o .,_, '\ • 4.;, t.1.~ .. DHS 3191 (Rt'viscJ 7/85) Soli,I ;rnJ Hazardous \Vastc (Review 7187) N .. C. Department of Hutnan Resources Division of-Health Services • • State Laboratory of Public Health P. 0. Box 28047 306 N. Wilmington Street Raleigh, 2761 I SAMPLE ANALYSES REQUEST Site Number -~N~C~D~~tJ_9~b~_+~~~'S~£~z~;~--Field Sample Number _4'--=-l_'3_/ ___________ _ NameofSite FC,)(-~r"9TESJ/'1 LL£ CollectedBy C. /o/1c1-toL.~ON ID# 3~ B-J,U, L,t._1,<r,1'l$ ' Type of Sample: • i Environmental ___ Groundwater ( 1) ___ Surface Water (2) __ Soil (3) _i__ Other (4) Concentrate __ isolid (5) __ !Liquid (6) I _·_'Sludge (7) I __ 1Other (8) Date Collected //ZS-- /-D 313T INORGANIC CHEMISTRY Extractables Parameter __ .Arsenic __ Barium __ Cadmium _._Chromium __ Lead __ Mercury __ Selenium __ Silver I Results mg/ 1 : ' Parameter• __ Arsenic __ Barium --------'-I __ Cadmium · --------'-' __ Chloride -------,-' · _·_Chromium·· ' __ .Copper __ fluoride __ Iron _·_Lead __ Manganese __ Mercury __ Nitrate -------------~' __ Selenium Results mg/ 1 Total Parameter __ Silver __ Sulfates __ Zinc _Ph __ . Conductivity _ms _TOC ·,. Results mg/ 1 ORGANIC CHEMISTRY P~rameter Results mg/ 1 _P&T:GC/MS __ Acid:B/N Ext. _TOX Parame.ter MICROBIOLOGY I __ (MF) Coliform Colonies/l00mls __ (MPN) Coliform Colonies/lO0mls 1 -- -- OateReceiv~-6-?9 VJ; Date Extracted -t{,-~ 1/P Reported By DHS 3191 (Rt"viscd 7/85) Solid and Hazardous Waste (Review 7187) I I I I I/A Parameter _EDB __ pews __ Petroleum -LEndrin _L_Linda11e X 'D,e id 'If\ Results Parameter __ Gross Alpha __ Gross Beta -- -- Parameter L Methoxychlor L Toxaphene 2,4-0 2,4 5-TP (silvex) Results PCi/ 1 .. .. Date Reported.,==,,--------------------ttE.:5 I , Date Analyzed :?--Z::-?'4-YP Lab Number ~p(};l,11_1. Chain of Cust9_ds Recore _·_Transp~~ _ Treatment -__ Si:orage Facility Disposfl-•*~;;~;~~Landfill · Locaticn of Sampling: Generator Facil!.t ;,(. Other: O#'-!>; le --. . .\ Company's Name . A/8 47 :-] £ /4-c-~=-'-'----'_ ~"-'--<='--4.::: .. -=-[ __ T_e_l--Je,p!-,h-ft:r· -e-(~-~2,---!~.C-)-.-'?->-ff"~'--+;4--C/_'6' __ , -\~ \. . -t4 G/ Address · / /0 /½ arl S~-7": s v, //.,,_ A>'<o.:.· ., 1c~~ #J · I / "7:ifi eRANCN ~"t!' Collect.or's Name . 4 e-=-I ,,,{,1y · f:::--.:-Tele_phoneey(/19,-,),.\GrvJ' 3'-2'&'"0 / '"{T"" [ signature 7 ;,t'2.Z , Date Sa,npled 3 ,t:::;, G 87'1 . Time S2.mpled / 3 z. / .:- Type of Process Generating 'l;laste FC.)( u.,a rc:h p-y,.,a-JL • ' --'--==-...:.=c..c...=====""----------,---- . Field Information· Fitld ~ample No. 1 Zt, 'f Chain c: Possession: 1. 2. 3. Res1.:l~s reported signaiz{,re! ' ' signature'' I signature, signat:urel I ; / z: s title title ti~le ,., J 2 - 3rd, '39-~kb o=J inclusive dates inclusive dates inclusive dates date lnst:-uct:ions: Complete all'. applicable inforcation incluciine; signatures~ and submit ..._-ith ·.analysis reques~ fo:-:::s. Receint fa:-S-=-=:il-es Tne samples described below were collec.ted i-;;-connection ••ith t:he administration, enforcement, and document:ation of 'the: () North Carolina Hazardous Waste Management Rules, 10 NCAC lOF ( ) North Carolina Solid •·wa~~e: Jtinagement )1'~ \ AF J V\) Comprehensive EnvironmentalH,esponse, I • ~ ; t• ! '( ••I !! • • • • ' ,':I ( ) Toxic Subs0tances Control .Act ,(tSCA). 15 Section 11 . of TSCA, ?--5 U .:si!c _-, § 2610. 't .,. .. .. Inspector_' s Name ;V}3 Ii) I LL..S Name of Firm SAMPLE · COLLECTED NUMBER DATE T-IME . i3 21 I ?F'Ef,9'/ . ...... ... I pc 3FE:€ Y~ /3 '2-4- Receipt for the above·· · s hereby SAMPLE TYPE WATER SOIL ·OTIIER { 0 t.1- -X· );iR._. X described. d: .._____ . Rules, 10 NCAC lOG Compensation and Liability Act (CERC-i..A) U.S.C. §2601, .~ ~-, specifically Inspector's Address DUPLICATE SA.\.fi'LES SA.'1PLE LOCATION ·· OFFER.El)IACCEPTED REJECTEDj oN-srn· OFF-SITI: .. . ' ,, , .. c., •.·· 'f.. ·.i .. X y.. 7--·· 1 ·X r I I I . . I Receipt/rejection of duplicate cir split samples is hereby ack.no.·ledged·: - Sign Inspector or Age:it : f/a/47 is/ Titl !it.le CO~NTS _________________________________________ _ Loc2ticn of Sz.npling: SOLID I DIVIS IO!, 0!' :iEJ..LT~ SC:?.\'ICC:S ~--..U.?J)OUS \.:ASTE :-'J.l;;_c~, ' Cn2.in of Cus::9~□"· Reco:-d Generator Storage Facility --1 ~O~her: tJI/-~ F2cil::.:: f?-a.rl : Company ' s Na.me __ -..::c!c::..:..,r.=<Z-e:.==-.,_/J,=-r--=d.=--"'2e--o="-'-=~=-==e::.·n-'--'~=c=----Tel eph one { jµSjh ) __ A./_D_...V_;;:f=:...... __ _ Address /6 3'0 Colle c ::or' s Na.me,_....:q,cC,...!::.~~ ::::......:,• /4).~~n-£!::k~· ,!.b-:=:..!:::::::.._ ___ Teleyhone ( 9 /9 ) ?-3'J'-Z B't> J V I signatuie ' Date S=pled __ ___.:::7::._...c...h-=-:/,::.....__.159"--',·---------~Ti.me S,:mpled )1')40 -ro /?4-?$ I of Process Generating ~aste._~A.'---'~"""-~)( __ ..::t,l).=-=a.=-re.=-~h-=-=-~-====----------- ' Type . Field Information-I· I I I Fitld S=ple No. -4 2 rt. +2-rt. y:._ I y:::_ C'oz.in ·cf Possession: 1. g- 2. 3. Res~::s reported signit:uR signature! I ' signature! sign2.t:ure I 4-Zr~ ;<. . ·Y-. ---re-. Y- '6 )'( ;>(._ ~ )(__ ' y,d?f-t ~ gy tit~e . inclusive dates title inclusive dates tit.le inclusive dates tit.le date lnst:-uctions: Complete ali applicable inforr:::.c.t.iO:-. incluC:ing signatures, and submit \..~ic.h;·.analysis request fo:-:::s. ' i ~ Comprehensive Environmental Response, Compensat:ion ~nd L:\.:i\:,j_li.1:y Act (CEizCL\) ( ) Toxic Substances Control Act (TSCA).15 /D.S.C. §26Ul, .'.:.E._ ~{-, speci.f:i.caJ.Jy t;~~::~~':::~::S C., 2610/ Inspecror: • s Name Ins pee tor, s Add Tess - SJ._'{?LE COLLECTED SAMPLE TYPE :t-.'mIBER DATE TL'1E WATER SOIL /01-~ .. 13+"f:, 2 jFEf;!'ffi '>(. ·. Receipt for t:he sample(s) described. above is hereby acknowledged: Sign{/;:::f £~,f c/~ OTHER ' II 1-ie I DUPLICATE SAHPLES I SAllT'.\...E LOCA'lION ' OFFEREDIACCEPTED REJECTED I ' ....... ., ON-';l'IT I OFF-SITE .. I t-~l X X ;( . ---- I I I i ' - ----. I I .. , ---------·------·---··-------- ------------------------- --------------------------------------------------... ., ______ -.. ------- Locc.t:ic~ of Sampl:i.ng: SOLID DIIISION OF H.EJ..LE SERVICES 1:--" • .li-.RDOUS \./ASTE !-'J.J,AGE:::EKT I C:oain of Cus::g_d'" Record CEIV£ -- Haz2rdous Waste.¥....aterials 1 AR llO f989 ,' § : . ~c Generat:or Transno::-:e p&;;AFl./r.reaulient: S F ili --D . l _ . ,. .... BRANCL•·•--~,._l t:orage ac t:y __ isposa :ac1..1.,.;t;Y.-., _ a:n:afill · --, -~:::.-~-- Fa c :iJ..::. t: x Ot:her: tJ#_ -µL --; ---""::;;-,r~=='-"-~----------------- Coo:pany' s Nrunefl..,.._, i Le-',--J;?a:,. k,-11 · /2µ,-,,f.,,_q Telephone(Wf:) ,g7 Z-1'r'l O Address $· /6,?,Y tue:rf ~-/ Sf. Sh2_/4-,.,.,,~ #C Z'j?~i'T Collec::or' s Name. _ _.:aa-:;,,:c,.,,...==-'-· ..:..U..:c..:~:..:.-=:..:•f-6..:-=-----Tel<cPhO':le ( '7/9 ) T 3 :$-2 ~I) I T I signat1fre Date Sampled. .? . h-~ I S"J. . Tilne S=pled / /" 0 2. ----'-"'-_;,...::;.:;;_~.::..,:...,__________ --'--'--.;;;._=------ Type of Process Generating Waste _ _,_,C-,......,C'=· ·LX'-__,W,::....c.cc¼J-=--==.::;~--=-=='------------- .Field Information ' Fitl6 Sample No. -?2?7... .<i 4-2 ?-CJ .'I 7---' ,< Ch~in cf Possession: 1. 2. 3. Res-.::~s reported 1Jd-1L signaturf I I signature_ signature signature I \ ·-. ! '. \ 4Z/i.9 X. ' . )'<. -,,,c : "'-,L. .. ·;,< ~-t< ,<. -,<. yfii i?-t-£f.8j. inclusive dates title inclusive dates tit.le inclusive dates ti~le date lnst:-uct.ions: Complete all applic2.ble infon:.ction incluCing si~at:ures, and submit ..... it.h ·.an2.lysis request fo~s. DI\'ISIOK 0: "=-!: -;-c sc-ov,c=-s ~ SOJ. AND HA.Z.ARDOUS 1-/J..S,:O: :'-!~'\.-',G~5;_:.J,CE .... :,.. . Receivt. :':o:-Sc.:::iles ' .::·:.. ' Tne sam?'1es described beio~ "ere collected i~-c:onnec:tion ,:ith t:he administration, ~ 1 \ • _. •y • l en ... orce.:::ienr, 2nd Gocumenta·t1.on of .:the: • ,,::;~1,•_·1-r·,._.1 { . ~ . . . ., .. • . :• .• "' ~1. I ( ) North Carolina Baz2c1id9.vs Waste Hanageme:1t Rules, lQ NCAC lOF ~ • • .., \ t .. ( ) No:::-th Carolina Soli(..f~ste Management Rules, 10 NCAC lOG 0Q Comprehensive Enviro=ental Response, Compensation and Liability Act (CERC-.c.A) ( ) Toxic Substances Control Act (TSCA).15 U.S.C. §2601, et~-, specifically Section 11.of TSCA, 15 U.S.C. ~ 2610. ; Grzove.a. /J,cHot..-r.oµ Inspector's Name Name of Firm Fi= °""-ner, Le-oAJ Op,,_;;atcr, or Agent k' 4/.J K: 1 A/ Inspector's Address Fi= Address · Title - SA..'1PLE . COLLECTED SAMPLE TYPE DUPLICATE SAMPLES SA.'1PLE LOCATION · NillIBER DATE TL'1E WATER SOIL -OTHER :3 ;? A:i3 'fl ilot. X· /J-112. - I I Receipt for the sample(s) described. above is hereby acknowle'7ed: I C AJ~ ~ .r-- OrrERED,ACCEPTED REJECTED! ON-'-SITE. OFF-SITI: .. .. X ' . X. x ,_., ' . I ... I Receipt/rejection of duplicate_ or split samples is bereby.ackno~ledged: . . Sig ture of Inspector er, Ope~ator, Or Agent :r. ~(lo fo7, -;-f ,. 1. L- , (O~KI S ;5;..,..,J Yc0 7U (-t> i-o SOLID clIV:SIO!, 0: F.:J-i.TE S:C:RVICES eE.-'-.2.L.?J)Q:JS \./ASIC: }"_!_l\AGEXENT ··cri _?,ecei:)~ £0::-Sa:ri"r>les ; a/ZC) {/£, /2 N1c1, 0 LS.o/v Inspecto~•s Name Fi=. Ow-ner, Ope~·a ::er, or Agent - SA.."!PLE COLLECTED ·sAMPLE TYPE lit™BER DATE TL'-!E WATER SOIL OTHER 4 lzFeB~ /IZS° .. )(_ .. /i 1£?_ . ------· ' . .. . ' . ' . - . ~ Receipt for the abov7 is hereby ,/ ,. .. sample(s) described. acknowledged: )J ;J,__. Inspector T~~ 1 qcc/4 ~ 7 ;,-j- . :· . -PT O:r v,·0·1 19,v Inspector's Add1:e$cs . ·, kiscJ•,1,€:">•·· \:: ·i:::.:.. -..... -· .... _ . ..;·'--------- Title DUPLICATE SA..l1PLES -~Ts,hl'.?LE. LOCATION . OFFEREDIACCEPTED REJECTED! ON-::::E l OFF-SITE .. . .. ' . I X X >< __ ......_ ___ . I ' . . ' ·-. I I __ _J_ I .. _____ L __ . Receipt/rejection 9f ch1pJ.ic_~t(~ ot !:iplit sampl·es is here:l:nJ .:.c.kno· ... J. e<lPt=d ·; VM".'b vJ · -~..,,-,._l1-:'. ::--,, --·-- ·sigzfa. r:ure of 'Firm 01..Jn::.(T, Opet";:: tor 1 or Agent ·{/· ;8/;.rvc/J. 111t1,...,i'H··cr-- Title ---·--------- CO~NTS ____________________________________ . _______ _ --------------------------------------···· .... -----·-·-· ------·- Loc:aticn of Sznpling: DIV:SION OF !iE.l-.LT:: S::C:?.VIC'cS SOLID -f_!.2.ARI)OUS 1/AST::C: ~J-J;AG:::3-:-6JICT! Ccasin of Cust9_d'" Rec:o:rc Baz2rdous ~aste H.aterials Generator Tr2.nspor:.e::- __ Storage Facility ..L_Other:--'~~~:::i&~---------\ Dis:,osal --. Company • s N2l!le 8.8 f r _ tlra,, cl. of/;~c c Address / 'l / 3 t{,k' r~-,=-;..12,..,_ -/ S-f!-. 5 -/4.. -/e .Sv 7 //e. ,1,/e,. Collector's N2l!le fl---/4)rvt_. /r--Teleyhone( C/1'1) ?-33'-Z'i'O/ signature/ Date Sa:npled 3 ,::::;,l, $9 Time Sa.mpled //ZS- Type_ of Process Generating Waste FCY tf_/~~ .Field Information Fitld Sample No. -? Z 9 3 X Chain c: Possession: 1. 2. 3. ' ' . a,.-, ,.,,_._ () Res.:::s reported signa t,tfre signature signature signature 4Z'l"I, Y- C: tl.'t.!.e title rit.le: 3 Fc.t 'l'l-~hi.7(1: inclusive dates inclusive dates inclusive dates Inst:ruc:tions: Complete all applicable info=astion including signatures, and submit \.:ith ·.analysis reques't fo::-::::s. ---------·---------· ------·--- ;Hazardous Waste Materials Locaticn of Sampling: Generator __ Transporte:-___ Treattnent Facilit __ Storage Facility __ Disposal ?acility __ Landfill· -15'._0ther: t2#-~ Company's Name,/1~ l Le_._ ,<?.a:,. k,-,, · 4<.,,kq Telephone (Wf) 'o7 2-1n 0 Address (ill. /6,?J t-ue rf F,-,L f>./. 5-k ks:,;,~ ,1/C Zf?ti'"?- Collector's Name'---'a-=:;,,'CL.C-==--=)/.=:~c..:-="-i'f-/....;.__=. _____ Telej,hone ( <?rl )_ .... '1-"3...:::!;...-....... 2::...:~;...l) ..... I.....__ T signatdre Date Sampled_. --'--J'=--'·"--h-=-'~--'=-1!9.._ ________ Tilne Sampled_..,_/_/''-C.O-=2."------ Type 0£ Process Generating Waste _ _,_F,_,C;·~X-'--_~?{A--'--'M-k4'-=-'==~~'-====------------ ' .?ield I:ifonnation :itld Sample No. '1277.... ·' 4-Z?'if :x Chain of Possession: 1. signature. inclusive dates 2. signature. title inclusive dates 3. signature title inclusive dates Res~l:s reported signature rit.le date Inst~uctions: Complete ·all applicable information including signatures, and submit: -,ith ·.analysis request: fon:is. DIVISIOK O? EE . .'.c. Tt' SE"i'.VICES SOLID ., .. m HAZARDOUS . eceint ::o:-Sa::"Jles ...::....·-Tne samples described below were collected in connection with the ad.ministration, enforcement, and ciocumentation of the: () North Carolina Hazardous Waste Management Rules, 10 NCAC lOF () North Carolina Solid Waste Management Rules, 10 NCAC lOG ~ Comprehensive Environmental Response, Compen~ation and Liability Act (CERC-.c.A) ( ) Toxic Substances Control Act (TSCA).15 U.S.C •. §2601, et~-, specifi_cally Section ii-o:f·rsCA, 1's·u:s.c. !l 2610. · ' '• ., .. -.. . ; Grz.ove: ra /JI c Hot..,oµ Inspector's Name Name of Finn )Jc .. .. : Inspector's Address Fire Address iYl-l!R'I ·kA-UK'!y OwA.102.. -9--04-'31:-Z-1-rio -:-_.:.;-::"':-;-:-:--::-::---'---------,~~=-==-='----'-----"--'-=c..-..:......,_..!::..;.;::___ Firm 0..-ner, Op7;;a~cr, or Agent Title L e-o N k' 4/.J K: 1 A/ S/...'1!'LE . COLLECTED SAMPLE TYPE NUMBER DATE TL'!E WATER SOIL OTIIER 3 J fi:T3 'if tlol. X 11,e Receipt for the sample(s) described. above is hereby acknowle~ed: C /l);::.)(,.__ , v--- Sign'aiture of Inspector Titfl:lo /4'? 7 ,f- DUPLICATE SA..11PLES SA..l-fi'LE LOCATION .·· OFFEREDIACCEPTED REJECTEDj ON-'-SITE. OFF-SITE .. ,, ?< :,. ;< . ' x . . I I I ---·~-.. I ... --. -· Receipt/rejection of duplicate or split samples is hereby. ackno-.,ledged·: .. . . -· Sigr.z.~u:-e of ·Firm_ er, Operator, -~ or Agent Locaticn of sa~pling: .. -------~ ------·--· ----------DIVISION OF EE..'-..I,T:: SE?.VICES SOLID. EAZ.ARDOUS \,'ASTE ~J-J;;.GE:S;,.CsJ/CE C"nain of Cus~r;td...-Reco:-d iH2z2rdous \.12ste !-'.E.te:ci2ls , I Generator Transporte~ __ Storage Facility f?71,r/ _Lother: tJ#-~ __ Disposal Facility __ Treatment Facil~t: __ Landfill · Co:npany' s N2me · c?r~.v 4,,-d ~ ';de:n ~ ~ Telephone(~) --=-'....::="--'=-"-=-==-~=~~-------------- Address /6.?o Collector' s N2me, _ _,,c;?,4,!.~,-,.~~::::._..t.,,U.~~c!-:::l:::_·+~~====----Tele_phone ( 91"1 ) 73';'-ZB'() / (/ signatufe Date Sampled_-=;?"---'R,,'--='-=~-... 1:)9'-'-_. __________ Time S~pled )IJ4 o -ro 174-'i5 Type 0£ Process Generating Waste FC)( tlJare. h~ ----'--"="----"--'-=-'--"=-c..C.....c===----------- . Fielci Infonnation Fiud S2mple No. 4 2 r/ 1-2-r(, Y--i-- Cnain c: Possession: 1. signature tit:~e inclusive dates 2. signature title inclusive dates 3. signature: tit.le inclusive dates Res~:~s reported siguatu±-e tit.le date Ins t:-uc tions: Complete all applicable. inf o~c :iO:--. incluC:ing signa cures, and submit. \..~ith ·..analysis request fo=-::!S. Tne saw?les SOLID l, ND li.;..Z.ARD O c S 9eceivt :o~ ._-_.-d esc rib ed belo~ ~ere collected in connection ~ith en£orce..:Jent, and documentation of the: .::he ad=.inistra tion 1 ( ) North Carolina Hazardous· 1..'aste lfanageDent Rules, 10 NCAC lOF ( ) Nort:h Carolina Solid Waste Management Rules, 10 NCAC lOG <;>4 Comprebensive·Environmental Response, cJmpensation and Liability Act (CERC'J...A) I () Toxic Substances Control Act (TSCA). llU.S.C. §2601, ~-~-• s.pecifically Section 11.of TSCA, 15 U.S.C. § 2610. YI' L. L tA./ It.-~ I ;<f-A/l ;S . . . . . . Cteovc~ f\/,cHol..!c-,v · Inspector.' s Name Inspector's Address Fin: Address Name of Firre ?'Riv l'r TE f2Es,, z::, c:-A../c_ ~- C,;::i IZ t. r;R.l'N-..::..:,u-ffl_::::_=.,12.'D"c---'--------'-· ~o'c-'l,(.J"="'-',v~e:...:/2=--------'-----'----Fin. _Cr..-""Der, ~p~:·2 tor, or Agent Title - SL'{?LE COLLECTED SAMPLE TYPE l\'mIBER DATE TTME WATER SOIL 10-f.e 13~ 2 JFEf?ifi )( Receipt for the saniple(s) described. above is hereby ackno~ledged: ~-CJJ.d.e~ Signaoce of Inspector / _ f?· /4 111.t- OTHER //II<. I I I I DUPLICATE SA..l'i?LES I SA.Mi>LE LOCATION OFFtREDIACCEPTED REJECTED I ON-SITE. OFF-SITE .. I X >< I I I I I I I I Tit.le . )( - of duplic2te or acknm,ledged·: 2 . split or Agent co~::-Zl~TS. ___________________________________________ _ DIV:SIOl-1 OF HU.LT:: SE?,VIC::S .,_ SOLID. E'.l.ARDOUS \/ASTE ~.1-J;;._G::'.::X:··;1!CB C~ain of Cust.9_ci.._. Recore I I Hazardous ~aste Materials Locaticn of Sanpling: Generator Transpor:.er __ Treat:rn.ent Fae..-,..-t __ Storage Facility __ Dis?osal ?acility __ Landfill L_Othe.r: ?'#-¼ Company's Name SB f T ,:1ra,1cl.. tJfl;~cc Telephone( n?f) ~rz-t;, S-'1-"B: Address I'/ I 3 me.r../-p;-9 ,.,_f S~ 5k./e.sv,r/-e A/e 2-fbt-1-- Collector's Name fj--· ;(),;;L_, / ~-Tele_phone( 9 l '[) ?-~ J'-C j'°() I signature/ Date Sa:npled 3 ,::;,, 6 't°9 Tine Sampled //ZS"""° Type. o:f Process Generating Waste FCX ~~~ .Field I:ifornation Fitlc Sample No. -?293 >< Chain of Possession: 1. signature 2. signature 3. signature Res~:~s reported signature 4-Z't!O y.. ,I 4Z'll · y.._ tit~e title title title inclusive dates inclusive dates inclusive dates date Inst:-uctions: Compi:ete all applicable infon;;2tion inclucing signatures; and submit \..Tith ·.an2.lysis request fo:-:::Js. ilIVlSION O? P.E.f..l.TS SERVICES SOLID . ,;n El-.2J3D0c1S \./ASTE y.;_1\J...GEXENT W'CE lieceio~ for Sc.:noles Tne samples described below were collected i~-connection with the administration, eniorce.ment, and documentation of the: ( ) North Carolina Hazardous Waste Management Rules, 10 NCAC lOF ( ) North Carolina Solid Waste !-'.anagement Rules, 10 NCAC lOG ()0 Comprehensive Environmental Response, Compensation and Liabirit:y Act (CERC'.i...A) ( ) Toxic Substances Control Act (TSCA). 15 U .S .C. §2601', .!:!. ~-, sp_ecifi'.cally Section 11,of TSCA, 15 U.S.C. § 2610. ; 0,eot/e/2· N1Cr/OLS-o/V Inspector's Name Inspector's Address BB/r Name of Firm /913 .tflle:;r ;::;,,,,,.rr · :5,. ~'S-,,,~;sv1LL£ AC i:$/.J~ Fire: Address Firm _0..-ner, Ope·::a::or, or Agent - SA."!?LE COLLECTED SAMPLE TYPE NUMBER DATE TL'1E WATER SOIL OTiiER 4 iZFeB~ /125" )(. lt11:?. Receipt for the above is hereby / - sample(s) described. acknowledged: /Jrvl, ature of Inspector (/cc/4 ~ 7;, -r Ti ::le Title DUPLICATE SA.l1PLES S.Aill'LE LOCATION ·· OFFEREDIACCEPTED REJECTED! ON-SITE OFF-SITE .. I I ,_. X X X . I I I Receipt/rejection of duplicate or split samples is hereby ackn "leciged: - Si f.aiure of Finn Own'±, Operator, or Agent ) ;gt,qr,/e,jJ. /)11'1 ,-/,q ~ Title CO~NTS, ______________________________________ _ ------------------· ·--------- DIVISION OF liEJ..LT::: S:C:RVIC:C:S SOLI~'D EJ..Z.ARDOUS \/ASTE :-'J.JU.G~♦!JICH Chain of Custg_ch Re·corc I Bazardous Waste Materials Locaticn of Sampling: Generator Transnorte:---. __ Treatment Facil::.:: __ Storage Facility __ Disposal Facility __ Landfill· X. Other: 0#'-1,;/e C0111pany's Name AIB /tl/lLS £'/c::,,,,,__ -~f.. .. .,.( Telephone(7of) -S?"3-'J4-9'15 Address /t'/t> h:.a.rl S~-:5-re&s,;::; //e.. A/C-2q&, r =?- Collector's Name._,,p.....e.e::-:::-c=:e.._---e.4.,.,.J.""-i,v(-"'-'-""~·-,c.h:----=....:..._;;; __ Tele_phone('J/9) 9 3' '3'-?FO / signature 1 /822 ' Date Sampled 3 ,I=;, 6 &'? Time Sampled 13 z_ / F -_ ___._::;__,_-"'-',::;_---'-.L-''--------------'-""'-'"'-'------ Type of Process Genera ting Waste _ _,Ac.....::<::'..=)("-. ---=-a,=a.=-n'-'=~:..f.:..:..o-..u==~==-------------• . . . Field Information Fitld Sample No. f 26 'f . f-Z: rO y:_ ?> :§..; ChEin cf Possession: 1. signature 2. signature 3. signature Res~l:s reported signature fZ.¥4· ?:? -~z?s= ; -< :::--;; - title title title ti~le / .><'-' J 5 2 - c'. ........ .----: = 2 -c__ r::::: • inclusive dates inclusive dates inclusive dates date Inst~uctions: Complete all applicable info~ction incluCing signatures, and submit ;:ith ·.analysis request fo=s. SOLID DIVISION O? EE-<.i.r:: S:C:RVICES I 'ID liAZARDOU S tieceivt fo:: Sc..::.::iles The samples described below·were collected i~-connection "'ith the administration, enforcement, and docUD1entat:.on of the: () North Carolina Hazardous Waste Management Rules, 10 NCAC lOF ( ) North Carolina Solid Waste Management Rules,· 10 NCAC lOG o() Comprehensive Environmental Response, Compensatiqn and Liability Act (CERC:-i.A) --. ·~ ( ) Toxic Substance_s Cont!ol .Act (TSCA). 15., 1./-~-C. §2601, .et~-, specifically Section 11.of TSCA, 15 U.S.C. Ii 2610. ·~ GRo vs:e . /J,c,-,o,_~ o,v. Inspecto!'.'s Naine Inspector's Address Name of Finn Fi= Address ,.UL z_~~r+- MfmEAA ~22-•~f!....:..L@'-L.!...8~tV-=-· __;.. _____ ~~~R~• ~,~~~C""--'-;~p~~'----~----~-D+~--~-~_1_-_S~~~7_S_ Fin,; _0..-ner, Ope~·a ~er, or Agent Title SA.'1PLE COLLECTED '.NU!-fBER DATE TL'1E I j PEf, 91 . J) ZI I pc 3F'El 'l~ '13 7..4- Receipt for the abov,e~:i,s hereby - SAMPLE TYPE WATER SOIL x X described_ d: OTHER to t..'L • . I ;q., f?_·' - DUPLICATE SA.l1PLES SA¾PLE LOCATION ·· ·orrEREDIACCEPTED REJECTED! ON-SIU. orr-srn: ,. .-,~ -"'"·,' . ' X y..· '7-- . Y-. I' X r . -, I I I Receipt/rejection of duplicate or ,split sa1:1pl.es is hereby ackno..,ledged·, l?M.ei/L tn' ~ - or Age::it Iit.lE C021!-ENTS~. ------------------------------------------'- I f· l r t r ' I I i ,. I l I l ,. ,, ,· YADKIN STR.£fT -r-N B9°-3o'w 4-88' 1-· LJ I, I, \) 'i-i-!,J I's: a: -I--\-, Ii) 1; ex: lt.1 _J ._j ' \} Vl f I 2;J llY ""'-5 2 Ii !JD ~ 5~9 ° -301 E N.5. MILLS S --5TATE5V/L PLOT PLAN l. SCA LE: (=60'-011 II. I 2 AGY"-5 s 4' '<t-i 0 , I Q \J) Nome of Admin. Un.it STATESVILLE CITY SCHOO LS -.,, . DRIVE. \!J~---~-----~ > -0.: Q 58'.9°-30' E 2.44° :J '-/• ·PEARL 5TREET . Nome of Building Home of School ) -5 88' -O' E. OUT POOR TENNIS BASKETBALL 34G.IS1 w~ f \,v(''i"' N. B. Mills Elementarv Schoo1. N.B.Mills Element0rv ~-"--Str•et Hame/tfo. 1410 Pearl Street Mai I Addro ss Statesvil l~. N. r 28677 " -7 I 1.9 I t,; ;; ~~ I ~, I I I i I I /'I 89°-5.:'j \ ~3-4' . I ; I \ I I 492-324 Unit and School Ha. Building Ho. ~'T i 2 •• FEDERAL . TRIP N O T I F I C A T I O N & A U T H O R I Z A T I O N TODAY'S DATE:~ PREPARED BY: /-:-. f% ,,IY}-: (Staff member filling out form) • SITE TRIP DATE OF TRIP: ,v/2,.1/£9 If trip date changed or cancelled note below: Cl!ANGE OF mTE TO: . OR CANCaLED:_· __ SITE NAME: ,,Cc: k < f/2 *~ NCD#: 0"15 -1-~ S2:/ REASON FOR TRIP: L;f',CZ7/ 6} &-p-::; /7;, -a,/ ~ CITY; 1/4_,fet,a Lle COUNTY: ~uf If Overnight trip, Hotel staying at: __________ _ Telephone Number: ________ _ ' (Please list appropriate county health person to call to advise of trip) ENVIRONMBITAL SUPERVISOR OR l-ffi'ILTH DIRECTOR TO CALL: ~ --1/'~ /J,etk.5 TITLE: b'lv1~rrcrtfa-(l/e4-d:fl._, . , Note 1f . , M.P., etc.) <Jif'Cr:fl<"r--c,..,fur- Tele])hone Number: (7cwl 8::,-2-5,3S,J> · · Project Team Leader: :]:b,q R/Q,o-f_C F:elt tZ.r2c,i<JT T\T Assistants: --------'--_,_7_7 __ 7 (V0vJ J 'ff--3931 AlITHORIZED BY: ATTA: TO NOTIFICATION FORM: 4 copies each of PRELIMINARY ASSESSMENT FORM NOTIFICATION FORM Staff Notification Procedure: (Use black {nk or Typewriter Only) 1. Above form goes to Data Management Coordina-tor (DMC) 10 days prior to trip 2. If date of trip. changes -note changed date; or mark "X" if cancelled 3. DAY AFTER TRIP submit to Lee Crosb a short ara ra h on site tri . .,I 17 ff-ti:li ~ Vt, Y~ d ,,1-~ h 1// ;Ji r.? A< ra Date: To: From: RE: 2 February 1989 Lee Crosby Grover Nicholson FCX-Statesville Air and soil sampling On 3 February 1989, Grover Nicholson of the NC Superfund Branch and Bill Williams of the Environmental Epidemiology Branch will conduct air and soil sampling at four to six locations around the FCX facility in Statesville. The sampling locations are at Mills School and at three to five other residential locations that surround the site. Samples of air will be taken using high volume particulate and vapor sampling devices. The samplers will operate approximately three hours at each location. Samples of surface soils will be taken at each location. The sampling program is designed to detect the present off-site migration via air of contaminants found in the soil on the site. These contaminants are primarily DDT, cholordane, and Dieldrin. Nicholson and Williams, as previously arranged will meet with Iredell County Health Department officials and with representatives of the Statesville City School System. Analyses of the samples will be done by the NC Laboratory for Public Health and the results should be available in 10 to 14 days, on or about 15 to 19 February 1989. FEDERAL TRIP N O T I F I C A T I O N & A U T H O R I Z A T I O N TODAY ' s DATE: 2 Fe-6 , 11 '19 PREPARED BY: 9 11....1,_:/= (Staff member filling out form) SITE TRIP DATE OF TRIP: ·. 3 Fq -g-"1 ., If trip date changed or cancelled note below:. ClIANGE OF !¥I.TE TO: . OR CANCELLED: --- SITE NAME: FC,X • ST"rTESVI LL.<::- NCDlt: 096 "1-55 52.~ REASON FOR TRIP: tfr/2 s1 £OIL s,4,1,t .PL1.U'1 C>Fr SI re CITY: Sr,t-~vn.1..~ COUNTY: 4,e'J>EL'- If Overnight trip, Hotel staying at: -------~---Tei e phone Number: ________ _ (Please list appropriate county health person to call to advise of trip) ENVIRONMENTAL SUPERVISOR OR HEALTH DIRECTOR TO CAL\,: @g -~"-//, St,~ek, TITLE:&,,_...;.t...i' /fe.,_J./t:._ ~~- Note if rlr., M.P., etc.) ' Telephone Number: (~o-f) ¥'1:'&·!i:~o>'. · Project Team Leader: ~ 1..;.,.;,l_-/,.__ Assistants:;// t<..,-;'lf>e,_..va _ t!#> Pe,/:;c-;-.,0__,,,, t:,,..,;,,....,......,._J..../._ o/;·. AIITHORIZED BY: ATIA!t.H '" "'" TO NOTIFICATIOO FORM: , 4 copies each of PRELIMINARY ASSESSMENT FORM NOTIFICATION FORM EPA TRAN MITTAL . r Staff Notification Procedure: (Use black -~nk or Typewriter Only) 1. Above form goes to pata Management Coordinator (IMC) 10 days prior to trip 2. If date of trip. changes -note changed date, or mark "X" if cancelled 3. · DAY AFTER TRIP submit to Lee Crosb a short ara ra h on site tri . ___:;,;11 l•'" .,.., ..,,.. ~,k. ~ rr ;/1; I kr -l>,A . 6 F A It 1AJ k1U11rvc~ ,Pr,,-,¥,-!f'!M. ,.0,..,,., J/M (1,1;//s )e41JDI January 25, 1989 TO: Lee ' ' FROM: Dave RE: Potential Inhalation hazard to community presented by chlordane contaminated soil from FCX Statesville site Based on the following calculations, it does not aooear as though the chlordane concentrations found in the soil at Fcx·present an inhalation hazard to the surrounding community. Assume: dust concentrations of 20 mg/m3 in the ambient air (this is twice the TLV for nuisance particulates and is so thick, people probably would not stay outside for long) 3; 1. 5 ('v.,rfs cit/or da'1,c, I or, p:,fs So, l , 11-Qc>e>OO.O. Q ;;),,3 Br ({ Lu~((t~-s ( &-Bra/le{) wo~(J ['/(e_ b Jo 4r >t?vwfv <t-50;1 ~f-OA7v<-.-td s/:-Jc:- ( fCVt1c~ralo/ (fi,o-vv/ .S~(} I ,. I \-----•· .. -, ·. I C~ '.Blue R,/~ ~H'~ ~ ~~ -~ &d_ !1%1/2~ ~ At~ ,, c/a/4 . • ~ -";;o9 ----------n--~~---~-- q7~t •_---------.r"""')----- --H------,--r✓-l --~ ~----- ~-++-----'-'-L~--=-------- ----tt-----=t--~-1 -- ~ -. ----~-~------ ---tt--______:~=--~__:0 1-----/ -~l - ; ; I , . ·'-' .,. --~~II fY(U'~ ?- '"-v"V,'1 h c-~ ,-_../ 0--6 ~ cu:-, c/'Z{_ /7/p ~ ar Tt3Y ~~-_ ~J ~~ 0 w11~·a,r)'}S 7b Jf:.<€ /'/ ~ ~~ r eiq ~k--_:~ ~ c;;r;?l~ ·. JM;.-, l • •. ;½e/?Ylr--) /✓ ~ fa U!!d W Jd!ci__ J~✓k~~~~ lu./?t,;~ . . I • 1//.S,-. /2~ ~ fa~'"7ZuJ 1-;f-t;--e_, /?-e~ lb ]10 t/v?b bdf ~~~ ;1~nA-e_ v~ -,--<-, ~ ~~/~ LJ k ~ j_ £f ~u1/11r /D I 7~ -7~ ~- ~ ~ -~/24~ r /~-P~/4~~w #~ .;_, vVJ4 /HJ fa f?eJ ' 7/ullk ' .. P~· ' 7),., 5t..,,..Js =, 9-3 "+ -~ 5"1 / tJC 'f>/-cde Pe.,,-?-. f.?es ~ cl<£ kb. '. --.. a . f ~1 4-IM~ ~ :::; '3 3 ~ -13' ~ t •· .. YI . fv.1 Cuc.fv-_ -1-j 1 -2 ,S-II , I "i""C','.) ,5 0 I crr..ro 40-0, - .. /l1.v1c,l,;;.,.,7 ~ J}_o T -5kwr r k_ l.. ... . ' - I , I ; '.{f~Jt" FF:DERAL TRIP N O T I F I C A T I O N & A U T H O R I Z A T I O N TODAY'S DATE: /q DEC. '$1 PREPARED BY: C:. µ,,J.. /s.,,..,-, (Staff member filling out form) SITE TRIP DATE OF TRIP: zo Dec. S'i3 E 3 "J"AlJ ~ -h, l3 J-f'I-..) '6"'\ If trip date changed or cancelled nbte below: OIANGE OF D\TE TO: ____ OR CANCaLED: __ _ SITE NAME: t=cx-S+d-esv,lle.. NCDII: 015' 458 SZ':1- REASON FOR TRIP: cPA R"'--f'f"\<>v"'-I o+ Sour<:_~ 0~ Cr,"+"'"'\"' ... ~"- CITY: :Srnresu11..1_.;,. COUNTY: 02Fr>tL-L_ If Overnight trip, Hotel. staying at: -----------Tei e phone Number: ---------- (Please list appropriate county health person to call to advise of trip) BNIRONMENTAL SUPERVISOR OR l!]g. tu,u,A-/>l D, MASH'iJveJ.J HEII.LTI! DIRECTOR TO CALL:~·· g lMSr TITLE: &uvr'/ /{eAL.Tf/ 'l:>tt2.e-LnR., · Note if Dr., M.P., etc.) Telephone Number: (::,c,q) 'i,~$ -°Tzq 1 Project Team Leader: b,,.., R IG<c. Eta Assistants: AUTI:!ORIZED BY: · AITA! l.)5 GPA TO NOTIFICATION FORM: 4 copies each of PRaIMINARY ASSESSMENT FORM (1st page only) NOTIFICATION FORM Staff Notification Procedure: (Use black -~nk or Typewriter Only) 1. Above form goes to Data Management Coordina-tor (D.'-1:) 10 days prior to trip 2. If date of trip. changes -note changed date, or mark "X" if cancelled 3. DAY AFTER TRIP submit to Lee Crosb a short ara ra h on site tri . , NOTES: HEAL TH DEPT. OFFICIAL CONTACTED: .:_fn:.:.;;.".:...' _,_lf7.:..!.!A_,_.,R.=,.;:.c.*:...:'2'=-"-ELT__,..,,.,e:.,,R:"-''K'"'--=€=--,L-"'~="'-''-'m""..e"'-'-'1 C!f" BACK UP LETTER REQUIRED: Yes No ._L :5"1--1 ILL-P,:,{2 -,e. J<. Y SHE;£K: I f2o,IJM-e;tJ77'r 1/I.QxR • 28 November 1988 'IO: File FROM: RE: Grover Nicholson FCX-Statesville I spoke on the telephone with Margaret &rrke; Iredell County Health Department, Envirornnental Section. She received a call from a resident who lives within one mile of the FCX facility and who is concerned about his well water. She wanted to know if we were going to do any sampling. I told her that the FCX facility is a proposed NPL site and that ATSDR will conduct a heal th assessment there. She said that she was requesting pesticide sampling bottles from the lab and would sample the well. GCN/pb/23 'IO: FRCM: RE: 26 October 1988 File Grover Nicholson 0J,J-rv{-/-- Citizen cornplainJ/ FCX-Statesville • Today I sp::,ke over the telephone with Darcus Kale of Statesville, NC, (704) 872-6298. She lives within a mile of the FCX facility in Statesville arxi has experienced health problems in the past. I explained to her the system of placing sites on the NPL. I also reviewed our site investigation arxi sampling results. I referred her to 01.uck Pietrochevitz arxi Cody Jackson of the Agenof of Toxic SUbstances arxi Disease Registry (ATSDR) , . (404) 347-3931. '!hey conduct health assessments on all proposed NPL sites. After talking with her she seemed satisfied that the state arxi EPA were taking proper actions at the site. GCN/pb/17 \ Well MWl MW2 MW3A MW3 MW4 25 October 1988 MEMORANIXJM 'ID: Lee Crosby FROM: Charlotte Varlashkin C..V RE: Trip Report for FCX-Statesville NCD095458527 • Stan Atwood and I visited the FCX site in Statesville on 24 October 1988 to sample the monitoring wells. We left for the site at approximately 6:30. We had to make a stop in Durham to pick up keys to the well. We left Durham for the site at 8:15 a.m. We arrived on site at 10:30. We walked around the site and took pictures. We began purging the wells at 11:00. Five wells exist on site. Only wells MWl and MW3A were sampled. MW2 was contained within a locked fence and not accessible. MW3 is the damaged well. MW4 did not have a bailer in the well. Samples were collected for purge and trap, acid/base/neutral extractables, and pesticide analyses after purging 3 well volumes using the dedicated bailers present within each well. We left the site at 14: 30. Samples were kept on ice until delivered to the laboratory on 25 October at 9:00. Water level measurements and field observations are outlined in the following table. Depth to Number of Volume Total Water Table Bailer Volumes of Volume Well from Ground Removed Before Bailer Purged Depth (ft) l Surface (ft) Sampling (liters) (liters) Observations 45.0 28.67 34 1.2 41 PVC bailer; slightly turbid water. 50.0 ND3 Unable to access well. 48.5+.5 2 33.00 50 0.7 35 PVC bailer; very turbid water. 49.5 32.75 Not sampled. 54.0 42.67 Not Sampled. 1. Information obtained from an Environmental Evaluation Report for FCX by Fred C. Hart Associates, Inc., unless otherwise indicated. 2. Based on field measurements. 3. Not determined. • 5 LI-f t:(1-///J) N. C. Department of H~r:nan Resouf~es Division of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Hca P. 0. Box 280 306 N.·Wilmington Str Raleigh, 276 Site Number 4 9 b a 9 5 'i S s,5 a 2 Field Sample Number ____ L/.:.._{_)_· -'9-~-=-------- Name of Site ---1---'-D--------------Site loca;ion ___ s_.:._/_·o;:;_l_:ce,c.:~=-e"c..LI.L'/-'/~ei;:.....------ 9 s Date Collected . . / c:J,/2 S<I '? r Time I l/: C,/J Collected By Type of Sample: . Environmental . ~ ___ Groundwater ( 1) ___ Surface Water (2) ' __ Soil (3) I __ Other (4) Concentrate __ Solid (S) __ liquid (6) __ Sludge (7) __ Other (8) /,r/ ,'~ Comm~ INORGANIC CHEMISTRY Extractables Parameter __ Arsenic __ Barium ~-Cadmium ___ Chromium _· __ Lead __ Mercury _·_ Selenium _,_Silver Parameter Results mg/ l Results mg/ l _ P& T:GC/MS. $EE ATTACHED SHEET( _· _ Acid:B/N Ext. _TOX -- -- MICROBIOLOGY Parameter __ ·_(MF) Coliform Colonies/lO0mls __ (MPN) Coliform Cclonies/lO0mls Parameter __ Arsenic __ Barium __ Cadmium __ Chloride _·_Chromium __ Copper __ Fluoride __ Iron __ Lead __ Manganese __ Mercury __ Nitrate. __ Selenium Results mg/ l ORGANIC CHEMISTRY Parameter L_EDB __ PCB'.s __ Petroleum __ Endrin __ Lindane Results mg/ l : :,, .. · Parameter __ Gross Alpha __ Gross Beta Total Parameter __ Silver __ Sulfates __ Zinc _Ph __ Conductivity _TDS -.. TOC. Parameter __ · Methoxychlor __ . Toxaphene _2,4-D __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Results mg/1 Results mg/I ,• Results PCi/1 Date Reported / O /3«,t:[ Date Extracted p Date Analyzed 10/n/~~~, O (0-,)7-i? 71-.u.r Reported By 1 /J d/,(,e-, Lab Number __ __c8 __ ,<i,_O __ o _______ _ DHS3191(Rev,s,d ~ ~~ J'O·-8'cJ7-c;:; [5S yvL ' M/1,c/m") N. C. Department of Human Resources Division of Health Services e SAMP1.,_E ANALYSES REQUEST State Laborarory of Public Hcali P. 0. Box 280' 306 N. Wilmington Stre Raleigh, 2761 Site Number _4'----'9~/)~0~9~S<---'-l---'--'5~,_5-'~S~ol..~---Field Sample Number __ -L_,_/_0::___:9_4,__ _______ _ Collected By Name of Site ;= C /\ Site Location 0 fa /e :C ,_, t /}e. --"'AC-L._f'--'-w'-"'o~o'--'c-=-'-f __ ID# __ L~/_5 __ Date Collected /o/J. '--:~/ '2e Time J '-/.' I 5' Type of Sample: E~rriental ___ Groundwater ( 1) Concentrate __ Solid (5) Comments _. __ Surface Water (2) ___ Liquid (6) __ Soil (3) __ Sludge (7) 'I.•' __ Other (4) __ Other (8) INORGANIC CHEMISTRY . Extractables . ' Total Parameter Results mg/1 Parameter " Results mg/1 Parameter Results mg/ 1 __ Arsenic __ Arsenic __ Silver __ Barium __ Barium _. -Sulfates __ ·Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead· __ Chromium ' --Conductivity __ Mercury __ Copper _TDS __ Selenium __ Fluoride ·--·----. __ TOC --·· __ Silver __ hOn ' -- --__ Lead -- --__ Manganese -- --· . __ Mercury --~.,. --__ N_itrate -- --__ Selenium -- ORGANIC CHEMISTRY ya;ameter Results mg/ 1 Parameter Results mg/ 1 Parameter .. Results mg/1 V P&T:GC/MSfiEEATTO.CHt:D SHt;;n(' J--EDB ,.':!! ··., ;,: ' _::...:..: Methoxychlor . , .. .. .. __ Acid:B/N Ext __ PCB's __ . 'foxaphene _TOX __ Petroleum _2,4-D --__ Endrin __ 2,4,5-TP (silvex) --· __ Lindane -- MICROBIOLOGY RADIOCHEMISTRY Parame.ter Parameter Results PCi/ 1 __ (MF) Coliform Colonies/l00mls __ (MPN) Coliform Colonies/!O0mls __ Gross Alpha __ Gross Beta .., ... 1 -c-·_ vf-7/i, Date Received ~''-'---'"'-----~'---""-'c....' --"--r'--· --~-------Date Reported-----~----------- . VDC.J ) 1J..,, Date Extracted Date Analyzed Ji:io/1& iJ ;}'l., _ , Reported By -..<if)r._,t'?::::\~~=----------------Lab Number B0..!b8l. DHS 319 I ( Revised 7/85) <' .. I: I --l IJ ____ .J-.. ~ \V/-~~a ('Q,..,,;,..., 7/P.7) Ru s h N. C. Department of Human Resources Division of Health Services SAMPLE ANALYSES REQUEST S~arc Laboratory of Public Hca\1 P. 0. Box 280' 306 N. Wilmington Stre Raleigh, 2761 Ljoq 0 Site Number _L/_"i_O~o~~Cj_5~'-J~5~?~5_;;>_._7~---Field Sample Number _ ___:=:::~~~~~------ c. . . Name of Site _ _,L_.::C==..,c,_... __ -. ___________ Site Location-. -~;)~~f-_q~~!~e~S:~v_'~/~/~'/~c~. ------ __ A-~l'-· -"'1,v~o~c,~J~--10# __ 4~·~5:~-Date Collected · / 0/d-~!/'i?f Time/ 9 .' Od Collected By Type of Sample: Envir~en-tal _V __ G G"'roundwater (I) Concentrate __ Solid (5) Comments ___ Surface Water (2) ___ Liquid (6) __ Soil (3) _. _ Sludge (7) __ Other (4) __ Other (8) INORGANIC CHEMISTRY. Extractables "• Total Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ 1 __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph ___ Lead __ . Chromium __ Conductivity __ Mercury __ .Copper _TDS . __ Selenium · __ Fluoride ·---0 TOC ·-··---- __ Silver -- --. -- -- _· _ Acid:B/N Ext. _TOX ~ .... Results mg/1 __ Iron __ Lead --. Manganese __ Mercury __ Nitrate __ Selenium ·,. ORGANIC CHEMISTRY Parameter , . Results mg/ 1 _EDB __ PCB's __ Petroleum VEhdrin ·£'undane 'f . .,, . o.--BHc MICROBIOLOGY ' __ (MF) Coliform Colonies/l00mls __ (MPN) Coliform Colonies/lO0mls Parameter __ Gross Alpha __ Gross Beta -- -------- -- Parameter Results mg/1 RADIOCHEMISTRY Results PCi/1 N. C. Department of Human Resources Division of Health Services SAMPLE AN AL YSES REQUEST . ,., . . ·-•j-_' •• State Laboratory of Public Heal . P. 0. Box 280• 306 N. Wilmington Stn: .. Raleigh, 276 Site Number _L)----'---'9_,.0~o_c;'---"5'--'L-/~· _s~· =?~5~°'~7 __ -Field Sample Number ___ '--/~C_J~Y_8~------- Name of Site ___ --.1..-_...cL=-=-----------,----Site Loca;ion. .5 f C1 I es t/.1 / / e_ Collected By _/j<.....;.-+f_c"',/"--"'O'--D=-""CJ'----ID# __ L-..,,/~5~· _ Date Collected -~/_0__,/~;;i__c_,_)_,_/_S:_..,_f'---Time Type of Sample: Environmental Vorouildwater (1) ___ Surface Water (2) __ Soil (3) __ Other (4) Extractable, Concentrate • __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) INORGANIC CHEMISTRY Para.meter Results mg/1 Parameter Results mg/1 __ Arsenic __ Arsenic __ Barium __ Barium _·_._ Cadmium __ Cadmium __ Chromium __ Chloride __ Lead __ Chromium •, __ Mercury __ .Copper __ . Selenium .. __ Fluoride.-. - __ Silver __ Iron --__ Lead --__ Manganese . · --. __ Mercury ~-,· --__ Nitrate --__ Selenium ORGANIC CHEMISTRY · Total Parameter __ Silver __ Sulfates __ Zinc _Ph __ Conductivity _TDS --_ . .TOC ---- -- -- -- -- Parameter Results mg/ 1 Parameter Results mg/ i' Parameter _P&T:OC/MS __ Acid:B/N Ext. _TOX _EDB __ PCB's _-_ Petroleum ....LLEndrin ethoxychlor __ oxaphene Results mg/ 1 _. ___ Results mg/ l <o.oo! · I /Tindane L -------------L,,/--;:;,,;~4-;_titiC ---:-;,1-D ...iL""":l,4,5-TP (silvex) -"'1!.!.~f.J,--¥,µf!!lJ~ A,lcoc, f'esf,<,',/fs MICROBIOLOGY Parame.ter __ (MF) Coliform Colonies/ lO0mls __ (MPN) Coliform Colonies/l00mls ·" '7 . Parameter __ Gross Alpha __ Gross Beta Results PCi/ 1 /, J -;.-9"'7 / ,~ Date Receivecl f. -,:x_) -/J O 1/ 1-· Date Reported . 'fl;-,;s-,. yP H0·\.) 'v1i),''0 ~\''j'l? ~ p~St. L--~Date Extracted /0-,:25-8'fr&w ,l"l::t':, -i.Olo<G DateAnalyzed 10 .. !.ii,~-ffi)7 {O-.:Z6:J'?V~ >Reported 1ly ~C,,-'----='----------------Lab Number 80Z{-;(3:J I ~ ,OHS 3 ! 9 ! ( Revised 7!85) ' I N. C. Oepartffient of Human Resources Division of Health Services • S-u ft: I\ F l.j SAMPLE ANALYSES REQUEST ' , . . ' State Laboratory of Public Heal P. 0. Box 280• 306 N. Wilmington Sm~ Raleigh, 276 i Site Number -l.f+-9--i·-o-o"---c~l-6~1./=f,~· ~7~· _s~·-~~l~----Field Sample Number ----"--'--"a'---'o"----------- Name of Site --~F_--_(._,~x~·-------------Site Loca;ion --~S~t~"'~J_-e..~2~11~1~!-~_e-ft>~----- Collected By -~A:~. _l~·-"'&,,,_/~o~co~c/'1-----ID# --01-+-=5~_ Date Collected __ f~O~/~;i_~'-)c--,,~),~g, ~\'-' __ Type of Sample: Environmental ~round water (1) ___ Surface Water (2) __ Soil (3) __ Other (4) Concentrate __ Solid (5) ___ Liquid (6) __ Sludge (7) __ Other (8) INORGANIC CHEMISTRY Extractables Parameter Results mg/ 1 Parameter Results mg/ 1 __ Arsenic __ Arsenic __ Barium __ Barium __ Cadmium __ Cadmium __ Chromium __ Chloride __ Lead __ Chromium __ Mercury __ Copper __ Sdenium __ Fluor::le. , ... ,. ___ Silver __ J.ron --__ Lead --___ Manganese --· -__ M~rcury ·-··· --__ Nitrate --__ Selenium .. ORGANIC CHEMISTRY Parameter Results mg/ 1 Parameter Results mg/ 1 . ~T:GC/MS _EDB Acid:B/N Ext. SE£ ATTACHED SHEET S) __ PCB:s _TOX __ Petroleum --__ Endrin --__ Lindane MICROBIOLOGY Comments Total Parameter _·_silver __ Sulfates __ Zinc _Ph __ Cond11ctivity _TDS ____ TOC -- ---- ---- -- . Parameter _·_ Methoxychlor __ Toxaphene _· 2,4-D __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Time Results mg/I Results mg/1 .. .. Para1ne.ter Parameter Results PCi/1 __ (MF) Coliform Colonies/lO0mls __ (MPN) Coliform Colonies/lO0mls /,, -J c-v71, /1'.) Date Received u ,:::: · _;:,-o (j / 1- J'.,/l, Date Extracted ID-.l/.,-$'? BD, 'fl\J Reported By@----------------- DHS 3191 (Revised 7/85) __ Gross Alpha __ Gross Beta Date Reported _________________ _ Date Analyzed / 0 <l 7 -f ~ /3 £1. Lab Number FI.QZGS'i¼ • N. C. Department of Human Resources Division of Health Ser.vices SAMPLE ANALYSES REQUEST ' ' ·.· .•• ,. ·).:_ . ,· State Laboratory of Public Hcalt P. 0. Box 2804 · ! ,·t•~-!306 N. Wilmington Stre . Raleigh, 2761 Site Number L/ 11 () 0 Ci 6. L1 r:: C/ .,c-"' 7 4· :,_ o , ---'--'.;__"'---'-I __ ~ )~::.>~4;,,--~2~°"~---· Field Sample Number ----~'~~c,,..~-------,---- Site Loca;ion :;$' l-ci f C s v,' )/e Name of Site ---!---'-'-"''---------------- ...,Ac...,__-__,1----""V'--o'-'--"o'-'c"',J~---ID# __ Lf~-~S~~ Date Collected -~jo~·,__/~d-_· '-1..,,,,.../~g_J~c·_ .. _· _· -Time I ':I; I s:::: Collected By Type of Sample: E:;r6nffiental · ___ Groundwater ( 1) I Concentrate __ Solid (5) ___ Surface Water (2) ___ Liquid (6) __ Soil (3) __ Sludge (7). __ Other (4) __ Other (8) Comments \ ~ -3A INORGANIC CHEMISTRY, , .,a,,.,-·· ... . . .. .. Extractables Parameter Results mg/ l __ Arsenic __ Barium __ Cadmium __ Chromium __ Lead __ Mercury · __ Selenium __ Silver -- --.. . --· -~-,- -- -- Parameter Results mg/ l z&T:GC/MS cid: BIN ExtSEE AHAGHEEl SI IEEf(S _TOX -- -- MICROBIOLOGY Parame.ter __ (MF) Coliform Colonies/lOOmls __ (MPN) Coliform Colonies/lOOmls Date Received /c:' -c"S:. ([;?' 1/1-0. Date Extracted f0-.:2(p-'('S' '13D,;,ffi, ';r\aj Reported By~ DHS 3191 (Revised 7/85) ,-••' • 11 ____ .J ____ \Vl--~n tO,..,;,.,., 7/fl.7) .. . Total . ' -~-. .. •.. Parameter •·-· Results mg/ l ', l .. Pa:rameter Results mg/1 __ Arsenic .. __ Silver __ Barium _·_Sulfates __ Cadmium .. ---Zinc __ Chloride _·_· •Ph- __ Chromium __ Cond_uctivity __ .Copper _TDS __ _.Fluoride . ---· _TOC •. . ·----. . __ Iron .. __ . Lead -- __ Manganese -- __ Mercury ' -- __ Nitrate -- __ Selenium -- · ORGANIC CHEMISTRY Parameter -"" _EDB __ PCBls __ Petroleum __ Endrin · __ Lindane Results mg/ 1 Paraffieter ·r.: Results mg/ l . .:·:•~·:.~. ·~ :.'..:.::. M~thoxychlor . .. ·-:,_•:.\, .. .. , . .. _. ·-· Toxaphene _. 2,4-D __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Parameter .. Results PCi/1 __ Gross Alpha __ Gross Beta Date Reported ________________ _ Date Analyzed / 0 -J. 7; f 'i 8 fJ Lab Number t30fZf&.8!5', JJ.i..Y.I_._,.,_.._, .. , ,._,,_ ___ .._._ • ...,-•••~--- SOLID M-p BA2ARD_OUS \./AS,T:': Y.J..l}AGlliENT BRANCH • The samples described below were collec,ted in connection ,,ith the administration, enfol'cemenr, and documentation of the:'""' ,:,:c~•J :·•· ~- () North Carolina Hazardous Waste Management Rules, 10 NCAC lOF () North Carolina Solid Waste Management Rules, 10 NCAC l0G -. . .. ( ) Comprehensive Environmental Response, _Compensarion_ and Liability Act (CERC'.c.A) ( ) Toxic Subsrances Control Act (TSCA)°, 15 U. S .C. §2601, ~ ~-, specifically Secrion 11,of TSCA, 15 U.S.C. § 2610. Inspector_' s Name . ' .. : Name of Finn ?inn Owner, 0pe-.i·a ':or, or Agent SA.'1PLE_ COLLECTED SAMPLE TYPE lllJ!-lBER DATE TIME WATER SOIL OIBER I ••• , ·. .. ,.,...,. -·- '--/092. 10/-;.'-f -Ffoo ✓--- {. ~. •• 0 °t '-f .... J'/-15 ✓ . ~-... -... . ---. 01" /lfOV ✓ 0 '18'. ' !'-I { 5 ,/ . --~ '_,;,:;,~: .:;f;. ·. . .• ... '. --· ... }:,(::· --~-<', __.__,_ 4100 t'{DO -✓ ;,, I . :'."' -l-//02_ ---.... -I f/C, --,:· __ ,J,., , __ -,., ... .... ...,._. •-·-........ ·. ~-... -----· P.eceipt for the sample ( s) described_ above is hereby acknowledged: Signature of Inspector Ticle .. I --/JC.. 'D .'.;. He-t If~ Ser0, UZ-d 1:J?.o. 7s¥ 2_09/ /2-/f:ler'J 6 _ Inspector·•-s Address Fine Addr_ess_ Tirle DUPLICATE SA.l-il'LES SA.l-fPLE LOCATION O?FtREDI ACCEPTED\ REJECTED I ON-SITE OFF-SITE .. I .. . , . ,,, .. I ., .. ~---· .... '• I I I .. . ' I -., . ::, \. '• ··-· ,< •,t-., _____ ---' ,. .,_ ... .. I I I Recei?t/rejection of duplicate or split sa□ples is hereby e.cknmdedgeci: Sig •. a~u::e of Finn O-~-ner, Ope::ator, or Ag 1.i.t.lE CO~NTS ______________________________________ _ ---------..•--------- LJ.LV.L.J.LU1\" ur ~..LJ..:. :i:..!',\'1-l,~:> SOLID AND HAZARDOUS \./ASTE l-'J._};JI.G::!-EKT ERANCH ,.Chain of cJ{laa,·0 ~ic:ir'a'·' . . . B2.zardous 1,12.st:e Hat:erj,al.s Generator Transporter __ Tre2.tment FaciJ. ' __ Storage Facility· __ -Iiispos2.l ?acility __ L2.ndfill Co.np2.ny Ts Name ____ )'------"'c"--. --'--x_· ___________ Telephone( ___ ) _______ ~_ Address S f 0 /es v"i J f.t. ·-----=-~-'--'-'----'--"--.;..:c::=-----'--"--------------------- Collector Is Nam·e .~; .:?'~ • . . . signature.-. · -- Time S2.!Ilpled Date Sa:npled /o la l/ /-e <i. .. ; . Type o:: Process Gene~a~~g-;-~~~.~-~~•;:~--5 / / C / cles •·· _._ __ .. /4;00 . Field l.:ifo~ation L/c< <;: :i. 4o93 Cn2.in o:: Pos;iessicin: 1. ~(Op 'f -10/2s ('it,~ signature, title inclusive· dates '~ ·~:,:. \ ' i ···•-.•·····' ·------"'-:-·-'.: ·-•·-:········~---··-·--·--------·-.. .., . . ···----...:.....----; ... ~~-· : (7 ~~,,ifZ a--,.,,JIY--=ZT: . I cJ ;,.zs0):i,' 2. ,,_ .. , ';. signature --~ •· ·. · --title .... ; --"·-inclusive-dates·: 3 . title inclusive dates Res~:is reported fYbe~~ signc.ture title Ins:~uctions: Complete all 2pplic2ble infon::ction including sign2t.ures, and submit. \.:it.h·.an2.lysis reques-c forc:s . • • • STATE LABORATORY OF PUBLIC HEAL TH -' ' Date of Analysis / /1/.:J/. /flfl ORGANIC CHEMICAL ANALYSIS . -7 --, DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES PO BOX 28047 306 N WILMINGTON ST RALEIGH NC 27611 Lab No. <,1n'1 /. ,i/} <;//)!) JO/ PURGEABLE COMPOUNDS MDL Field# LZ 12-·1.J.oq11- -Tv= r I l r , 1 - ----···-ll-! L.:. £all J ,n/Cn /411 L -"·- Dichlorodifluoromethane I .~!. -Uf-Chloromethane {Vinvl Chloride Brananethane Chloroethane ' Trichlorofluoromethane 1 / fl. 1-Dichloroethvlene ~' )(' _11ethvlene Chloride . J tert-Butvl Methvl Ether (Transll 2-Dichloroethvlene -· -~s l ether _ l_, 1-D i ch l oroe thane , IYl 2.?.-Dichlor=r=ane l ~/Cisl l 2 Dichloroethvlene I, /,, /, 7 ·1 Chloroform _ JBCMl Braooch l oromethane ·11 ✓l. l. l Trichloroethane Li, I; l l Dichlor=ronnne u... {Carbon Tetrachloride i k' {Benzene 1 - ✓l 2-0ichloroethane Jk ,;;. {Trichloroethvlene 1.2-Dichlor=rnnane I -· Braoodichloromethane Dibraoomethane Toluene +..-JI, .0 1. 1.2-Trichloroethane u -Tetrachloroethene /,:iq _J_.3-Dichloronr=ane I Dibraoochloromethane 1,2-Dibraooethane (EDB) __ I-Ch l orohexane \ I ' I . ' .. - - COIIIIENTS : ?T/&c.,/ /V[j. ' C!~'vrYJ~e_c:L ~-0_e_,ric.2- J .. Estimated value. . K ... Actual value is kna.m to be less than value given. L -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. NA .. Not analyzed. 1/ -Te.ntative identification. MUL -Mininun Detection Limit for water (EPA Method 502.2), µg/1. ✓ .. He~ulated voe . T -Tr1halomethane N.C. Division of Health Services OHS 3068-0 (4/88·Laboratory) 0--- '' . ' \ I I 1. ·1 ' ; ' ,J LI • ' f l r l ( l --/1 ·" •• ,., I l • ,,., 11.,,., .. n,l ... ,en --· - .. . • STATE LABORATORY Of PUBLIC HEALTH - DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON ST, RALEIGH, N.C. 21611 ORGANIC CHEMICAL ANALYSIS Lab No. )( n rJ,'/ ✓Pl ) 'l(ll'II SI PURGEABLE COMPOUNDS MDL Field# 4-ofz,,, l.f09'f Tvne ( }. ) ( I) a=•~,.,~ I lni tc ~,<71 , ..... JI,,,.. Aon/] ).a/l,a -Ch lorobenzene I /l" h II Ethvlbenzene If _l.1. 1.2-Tetrachloroethane _p-Xvlene m-Xvlene o-X~lene Stvrene Braooform Isl"lnrnnvlbenzene .J.,.1.2.2 Tetrachloroethane Braoobenzene _n-Propvlbenzene 1.2.3-Trichlorl"V"lrnn.~ne -2-Chlorotoluene -1 3.5-Trimethvlbenzene -4-Chlorotoluene (Tert) Butvl Benzene Pentachloroethane 1 2.4-Trimethvlbenzene (Sec) Butvl Benzene _D-Isooronvltoluene l 3-Dichlorobenzene ✓l 4-Dichlorobenzene n-Butvlbenzene l 2-Dichlorobenzene _(Bis) 2 Chloroisnn..,,,,vl Ether _l.,_2-Dibraoo-3 Chlo ne I _l_,_2 4-Trichlorobenzene I ' Hexachlorobutadiene Naohthalene I . l... 2 . 3-Tr ich l oroben zene ; I \ , I - J -Estimated value. K -Actual value is knowa to be less than value given. L -Actual value is kno,,n to be greater than value given. U -Material was analyzed for but not detected. NA -Not analyzed. 1/ -Tentative identification. MDL -Minimum Detection Limit for water (EPA Method 502.2), µg/1. ✓ -Re~ulated voe l -Tr1halomethane N.C. Division of Health Services OHS 3068-0 (4/88 Laboratory) v-- ./ ( ) ••"1/1 ,.,../L,n .. - ( ) ( ) .. nil ,,n/L.n ,nil 11n/Vn BASE/NEUTRAL AND ACID EXTRACT ABLES COMPOUND N-nitrosodimethvlarnine bis(2-chloroethvllether 2--chloroohenol ohenol 1,3-dichlorobenzene 1.4-dichlorobenzene 1,2-dichlorobenzene • STATE LABORATORY OF PUBLIC HEA- DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES P.O. BOX 28047 --306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS LAB NO fJO?-ufl<i 11 O ? /,.C,_'5. FIELD# 4/00 LJ,1 0 2-- TYPE < I l C I l ( ) ( ) UNITS ,ua/1 ,,,,.,.,,., rua/1) ua/1 ua/ka un/1 un/ka JI\/ -1:JO If.--l,L bis(2--chloroi llether hexachloroethane N nltroso--di-n-nrnnvlamlne nl trobenzene 1 <:IV'lhorone 2--nitroohenol 2 4-dimethvlohenol bis(2--chloroethoxvlmethane 2 4-dichloroohenol 1.2.4--trichlorobenzene naohthalene hexachlorobutadiene 4--chloro-m--cresol hexachlorocvcl"""ntadiene 2,4,6--trichloroohenol 2--chloronaohthalene acenaohthvlene dimethvl ohthalate 2.6-dinitrotoluene acenanhthene 2.4-dinitrnnhenol 2 4-dinitrotoluene 4--nitroohenol fluorene 4 chlornnhenvlohenvlether diethyl ohthalate 4 6-dinifro-o--<:resol diohenvlarnine azobenzene 4--bromohenvlohenvlether hexachlorobenzene =ntachlornnhenol phenanthrene anthracene dibutvl ohthalate fl uoranthene J --Estimated value. SO//hSO 10/.?'?o "0/;t.,C:O /0/11.30 I J, soiuxr j,, / /l 1.330 1~1:,~~ SOl/t.5'0 /t)/ ?30 \' ,n1) L H .. o/so11 ..... .- 'I K --Actual value is known to be less than value given. •/ ( ) un/ 1 un/kq . L --Actual value is known to be greater than value given. U --Material was analyzed for but not detected. The nurber NA --Not analyzed. • is the ~inirrun_Qetection !:_imit. m])L 1/ --Tentative identification. g; --On NRDC List of Priority Pollutants. ~V,i.,v.u..-<.an 06 f/ea.lth SeJl.v,i.,c.v, Vf/S 3068--0 (4/86 LaboMtotty) - ( ) un/ 1 un/kq •. STATE LABORATORY Of l'U8LlC HEALTH O!V!S!OO Of HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOUHCES P.O. BOX 28047 -306 N. 1,/[LHINGTOO, SI., IVILE!GH, N.C. 27611 ORGANIC Q;EM[CAL ANALYSIS BASE/NEUTRAL ANO ACID LAB NO r;((.17/A~J'-/ Yo.a&Fi(- EXTRACT ABLES FIELD# i/11,n L//02- aJMPOUNO TYPE ( I l c I 1 r. ) ( ) UNITS /" 110/ 1 I un/ko /un/ i)un/ko uo/ 1 un/ko uo/ I uo/ko ovrenc /0/.~"l/'I tL-.(__ benzidine .-s-n /11,,so butvl benzvl ohthalate JO, '130 benz(a)anthracene chrvsene . , 3,3---<lichlorobenzidine so/lh5o bis (2---ethv I hexv l ) ohtha late l/n/330 di-n-octvl ohthalate /0/.130 benzo(blfluoranthene so/th'>O benzo(k)fluoranthene benzo(a)nvrene i ndeno ( 1 . 2 3--ed) nvrene dibenzo(a h)anthracene benzo(o h. i)N>rvlene \ , .... .I ' I aniline s" 0 /J 1,, "'O £..\.... \.,L benzoic acid benzvl alcohol . , 4--eh loroani 1 i ne JO 330 dibenzofuran 2--rrethvl n.anhtha 1 ene 2---rrethvl oheno 1 4--rrethvlohenol ~:, 2-nitroani 1 ine S-o r,1.,;o 3-ni troani 1 ine 4-nitroaniline 2.4 5 trichloroohenol \/ ,, \ / m 1) 1- J -Estimated value. H 2. 0 / Soli... to be less than value given. to be greater than value given. K -Actual value is known L -Actual value is known U -Katerial was analyzed NA -Not analyzed. for but not detected. The nUTber is the Hininun Detection Limit. l/ -Tentative identification. 2/ -On NROC List of Priority Pollutants. ~ Div;./2-<.011 06 fie.aUli SVtv-<.c.v., OHS 3068-0 (4/86 Labona..to~y) ( ) ( un/ I uo/kQ ,,o/1 u V N. C. Department of H~man Resoufces Division of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Health P. 0. Box 2804 7 306 N. Wilmington Street Raleigh, 27611 Site Number __ 4-'-_9'--'b"-'a"---'-9--'5"--_,_i~5_,c?__.,..,_5~a"'-2,___ Field Sample Number --=----,-Lf-'. _l_J_·-'-9-~-------- Name of Site --..J...--'-c,_ _____________ Site )..ocaiion -,---S-~/_o_l~e.~s--~v~tk'l~J~e-=-------- Collected By -,-, A~-'f--'/:k'.~O~o~c=J~--IOI/ 9 5 Date Collected. /CJ,/a l,;1¥ r Time I l/:tJo Type of Sample: Concentrate Comments __ Solid (5) t I ___ Surface Water (2) ___ Liquid (6) __ ·_ Soil (3) __ Sludge (7) __ Other (4) __ Other (8) INORGANIC CHEMISTRY Extractables Total Parameter Results mg/ l Parameter Results mg/ l Parameter Results mg/1 __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _ms __ Sclc::nium __ FluoriJe -------___ Toe __ Silver __ Iron -- --__ Lead -- --__ Manganese -- --· -__ Mercury -- ~ ... --__ Nitrate. -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Results mg/1 Parameter Results mg/ l Parameter Results mg/ l t,," P&T:GCIMS SEE ATTACHED SHEET( 1--EDB __ Methoxychlor __ Acid:B/N Ext. __ PCB:s __ Toxaphene _TOX __ Petroleum _2,4-D --__ Endrin __ 2,4,5-TP (silvex) --__ Lindane -- MICROBIOLOGY RADIOCHEMISTRY Parameter Parameter Results PCi/1 __ (MF) Coliform Colonies/lO0mls __ (MPN) Coliform Colonies/l00mls __ Gross Alpha __ Gross Beta Date Received ~/~· · __ ; _ .. ~-·•_ .. _._-_::;_~:_~--_;_'/_-,~_., __________ Date Reported _________________ _ v•'--/ l Date Extracted -~----------------Date Analyzed 1cp1,1 "rf~~™,, .. f'R~~~ft~:~· ,{'e:su /;r~ ,f;J_A,i?;z;=._. Lab Number 80~6o0 DHS319l(Rev;sed7/8S) #:f"c:J 2-&YtJ-S::07,~y_s;- Solid and Harnrdous Waste (Review 7 /87) 1/ N. C. Department of Human Resources Division of Health Services • SAMPLE ANALYSES REQUEST State Laboratory of Public Health P. 0. Box 2804 7 306 N. Wilmington Srreer Raleigh, 27611 Site Number _4'---'9---'-'/)'----"0e-9c...=5e-'--/~5e-S°~S~a~---Field Sample Number _1-/~_0 __ 9_l..f~-------- Name of Site -~F_-_-_C~-~i(~--.------------Site )..oca;ion . 0 fa le :( 1;,, , "l/<?e -~A~~) ~w~o~c-~cJ~--ID# __ '-_/_5 __ Date Collected / 0 / 'd '-;~/ r;., K Collected By Type of Sample: Concentrate Comments E~mental . ___ Groundwater (1) __ Solid (5) <11 ;,v ,i A __ Surface Water (2) __ Liquid (6) __ Soil (3) __ Sludge (7) __ Other (4) __ Other (8) INORGANIC CHEMISTRY Extractable• Total Parameter Results mg/ l Parameter Results mg/ l Parameter . __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead· __ Chromium __ Conductivity __ Mercury __ Copper _TDS __ Selenium __ Fluoride --· __ TOC __ Silver __ Iron -- --__ Lead -- --__ Manganese -- --· ----__ Mercury -- --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY .,Parameter Results mg/ l Parameter Results mg/1 Parameter v P&T:GCIMS SFE ATTACHED SHEET( +-EDB __ Methoxychlor __ Acid:B/N Ext. __ PCB's __ T oxaphene _TOX __ Petroleum _2,4-D --__ Endrin __ 2,4,5-TP (silvcx) --__ Lindane -- MICROBIOLOGY RADIOCHEMISTRY Time J 'f ,' I 5' Resu Its mg/ l --·· Results mg/ l Parameter Parameter Results PCi/ l __ (MF) Coliform Colonies/!00mls __ (MPN) Coliform Colonies/ IO0mls __ Gross Alpha __ Gross Beta Date Received ~· ~"-·_· ,_. __ /;_,_:·~7_;r_,_.,,_, __________ Date Reported _________________ _ Dare Extracted __________________ Date Analyzed vo5-p,Jar, 7!'!;1, -, ·" Reported By Lab Number gQ.-;.l,8~ OHS 3191 (Rev;sed 7/85) Solid and Hazardous Waste (Review 7/87) I ! ' N. C. Department of Human Resources Division of Health Services SAMPLE ANALYSES REQUEST Rush State Laboratory of Public Hcalch P. 0. Box 28047 306 N. Wilmington Streer JICJQ c::....· 7 / cc, Raleigh, 27611 Site Number _L/_'1'--Q~Q""---'Cf_5"-'-J-'--5~· ~"--5=--c,;i_'---'7'------Field Sample Number-~:::~~"!:':~"-------- Name of Site ---'------'c~U,....-----,------------Site Locaiion -c-. -~s~~~~q~~i~e~s:~v-~I~·~; l~e.~-~------ __ A-'-'-l--=IN'_o~· -"-D~Jc...._ __ ID# __ 4~,~5: __ Date Collected · / 0 1/-2, LJ)'Z R'. Time / 9 .' Od Collected By Type of Sample: Envir~ental _V __ r. G.,roundwater ( q Concentrate __ Solid (5) Mv Comments ___ Surface Water (2) ___ Liquid (6) __ Soil (3) __ Sludge (7) __ Other (4) __ Other (8) INORGANIC CHEMISTRY Extractable• Total Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ 1 __ Arsenic __ Arsenic __ silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _TDS __ Sele1iium __ Fluoride --__ TOC ---·•----- __ Silver __ Iron -- --__ Lead -- --__ Manganese -- ---~---__ Mercury -- --__ Nitrate. -- --__ Selenium -- ORGANIC CHEMISTRY Results mg/1 Parameter Results mg/ 1 Parameter Results mg/ 1 __ Acid:B/N Ext. _TOX Parameter MICROBIOLOGY __ (MF) Coliform Colonies/lO0mls __ (MPN) Coliform Colonies/lOOmls _EDB __ PCB's __ Petroleum vndrin __ Lindane Parameter __ Gross Alpha __ Gross Beta RADIOCHEMISTRY Re~ults PCi/ 1 Date Receive'/-,.::::::=-~--·~•-_,~_-_"_,.-:::-"i:-:;'.'._'·,...-:;_-:---,---,s-c--=~---Date Reported --,-----===---------- t-1,,rb (\·\GD t-le.,·b . __ 'f'e"ST ~""--><>--"'---'-'-'-'-h..---''-'-. ",µ;Cf~'-c_·.,_1'"''\~,.,·'"", _____ Date Analyzed i ,A.i7) 0 ~---f';, ;:l JO-.2(,-ifYJ:i -----------------Lab Number 80Zft>82 Reported By DHS 3191 (Revised 7/85) Solid and Ha:ardous Waste (Review 7 /87) ' --- N. C. Department of Human Resources Division of Health Services SAMPLE ANALYSES REQUEST Seate Laboratory of Public Health P. 0. Box 28047 306 N. Wilmington Street Raleigh, 27611 Site Number _L)-'---'9'--""D'-=O~C/<->,5"--'L/'----5..,_· S".~.SL-"'o<'---'-7 __ Field Sample Number ---~--'--"{J:........:.°f....:1>=---------- Name of Site ----'---__ L_,c..:..._--~------Site )...oca;ion -. -~SL-.;...l.....::::Ct!c...!...l..:cec.,;s=....:1/:.....:.J_/,..:./_e.=------- ----'A'--'-_f'---"-,,'"'-/---'0"--'='0'--"'C;)'--__ ID# __ L-.,,_,J_,5..,___ Date Collected --'-/_o"--f/_cJ.=-_c;'-'/c.....;:;s-,----"-(f_ ,Time Collected By Type of Sample: Environmental Concentrate V Groundwater (I) __ Solid (5) ___ Surface Water (2) ___ Liquid (6) __ Soil (3) __ Sludge (7) __ Other (4) __ Other (8) INORGANIC CHEMISTRY Extractables Parameter __ Arsenic __ Barium __ Cadmium __ Chromium __ Lead __ Mercury __ Selenium __ Silver ------. ---- Parameter _P&T:GC/MS __ Acid:B/N Ext. _TOX Results mg/ I -- Results mg/ l MICROBIOLOGY Parame'ter __ (MF) Coliform Colonies/ IO0mls __ (MPN) Coliform Colonies/lO0mls I _} i-~ c--,7 ,., ,,..,..., Date Receive~ :'. -._;<__; -ri :, ·1,/ /-·· ff.rr: -yp Date Extracted /0 -;JS:-BKEJJ'' Total Parameter Results mg/ l Parameter Results mg/1 __ Arsenic __ silver __ Barium __ Sulfates __ Cadmium __ Zinc __ Chloride _Ph __ Chromium __ Conductivity __ Copper _ms __ Fluoride. -------_TOC . __ Iron -- __ Lead -- __ Manganese -- __ Mercury -- __ Nitrate -- __ Selenium -- ORGANIC CHEMISTRY Parameter _EDB _PCB'.s __ Petroleum _ 1 /F ydrin ---1.L1..indane Results mg/1 Parameter Results mg/1 ethoxychlor __ oxaphene _z 4-D · .C:O.CO ~4.5-TP (silvex) "-0.CO { ---'-"''--l-::Ll4.!1!1.J __ L/f"_ C h lo c, f'e < l'--'''-'·(.,_·,..c·,1wf-->..£ ___ _ Parameter __ Gross Alpha __ Gross Beta RADIOCHEMISTRY Results PCi/ 1 Reported By _________________ _ DHS 3191 (Revised 7/85) s,~li,I ,.n,~ H,.,,.rrin,1c; Wure (Review 7 /87) I i N. C. Oepart"ment of H~man Resources Division of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Health P. 0. Box 28047 306 N. Wilmington Street Raleigh, Z 76 I I Site Number -Lf+-9-l. . ...JQ!,,l-.:eO:._.,':f-"-5-~.,_,_.C,,_· ..,?,_· ....,S"-"~=--<7 ____ Field Sample Number---~~{)_._(] _________ _ Nome of Site __ ..,_f_-...c{.:..._-')(..,_ ____________ Site l.-ocaiion ~---"S"-'f'--"'a~f...,-e.~5=,;_,1_,_/_,_/.""e..,~"'------- ~M~~f~l!~l~P~C~2~c ..... / ___ ID# --0!+-=5 __ Date Collected _....,_[_c;_0_,1--).e:.a:...'1-1-+,/-"'?--'-?_· -Time ~/_9_,__: o~O~- Collected By Type of Sample: Environmental doroundwater Concentrate (I) __ Solid (5) __ Surface Water (2) ___ Liquid (6) __ Soil (3) __ Sludge (7) __ Other ( 4) __ Other ( 8) INORGANIC CHEMISTRY Extractables Parameter Results mg/1 Parameter Results mg/ 1 Comments Total Parameter Remits mg/1 I __ Arsenic __ Arsenic __ Silver I __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _TDS __ Selenium __ Fluor:Je -___ TOC __ Silver __ Iron -- --__ Lead -- --__ Manganese -- ---__ Mercury ---·· --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/1 ~T:GC/MS EDB __ Methoxychlor d:B/N Ext. SEE ATTACHED SHEE LPCB'.s __ Toxaphene _TOX __ Petroleum _2,4-D --__ Endrin --2,4,5-TP (silvcx) --__ Lindane -- MICROBIOLOGY RADIOCHEMISTRY Parameter Parameter Results PCi/1 __ (MF) Coliform Colonies/l00mls __ (MPN) Coliform Colonies/!00mls __ Gross Alpha __ Gross Beta I, ,,, __ ~/ ,/ Date Received ~;_:--_·,_,,_· ·_· ·_-_._·~~•,.,·· ,..;~(!_!_'.) __________ Date Reported _________________ _ M n Date Extracted ID-.J.1.,-'.r? Bu 11\i.J ,. Date Analyzed JO-;:l. 7-f ~ /3 t:,J.. Reported By DHS 3 I 91 ( Rev;sed 7185) SoliJ ;rnJ Hazardous Waste (Review 7187) ' N. C. Department of Human Resources Division of Health Services • SAMPLE ANALYSES REQUEST Seate Laboratory of Public Health P. 0. Box 2804 7 306 N. Wilmington Street Raleigh, 2761 I Site Number _L._,/_Cf_;_=..{)_O_q'-----'-6_½~1J"---<S,,,--ufScc;;).cc..--7 __ Field Sample Number __ 4--'---"f_C_,--'c)_"----------- Name of Site -( Site Loca;ion. :$ fc1 f CS v,· )/e Collected By ...;,A-'--'--'-j---'V:""--'Q'-Q""--'-Cq..,/ ___ ID# __ L/~5~-Date Collected -·~/o-/~d-~'-/_,,./--'<8''-"X:::---Time I '-I ; I S:::: Type of Sample: E7nmental ___ Groundwater (1) Concentrate __ Solid (5) tv -3A Comments __ Surface Watet (2) _· __ ·_ Liquid (6) __ Soil (3) __ Sludge (7) __ Other (4) __ Other (8) INORGANIC CHEMISTRY Extractables Total Parameter Results mg/1 Parameter Results mg/ 1 Parameter Results mg/ 1 __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _TDS __ 5elenium __ Fluoride _TOC --·--- __ Silver __ Iron -- --__ Lead -- --__ Manganese -- ---· ~.,. __ Mercury -- --__ Nitrate. -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ 1 l7A~T:GC/MS . _EDB __ Methoxychlor cid:B/N Ext. SEE IIIlACl:lEO Sl:lEET SJ--PCBls __ T oxaphene _TOX __ Petroleum _2,4-D --__ Endrin --2,4,5-TP (silvex) --__ Lindane -- MICROBIOLOGY RADIOCHEMISTRY Parameter Parameter Results PCi/ 1 -. _ (MF) Coliform Colonies/!00mls __ (MPN) Coliform Colonies/lO0mls __ Gross Alpha __ Gross Beta Date Reported _________________ _ Date Analyzed JO -J-7-ff f,fJ Reported By _________________ Lab Number 8tl>Zi&B:5, DHS 3191 (R,v;sed 7/85) SoliJ and Hazardous Waste (Review 7/87) I SOLID ~DUS WASTE l-'J.JiAG2£KT WCR Chain of · Custoch· Re·c·ord Bazardous Waste l:1aterials Loca:icn of Sampling: Generator Transport.er __ Trea=e.nt Facili·. __ Storage Facility __ Disposal ?2cilit:y __ ·._L2.ndfill Co.np2n·y's Na.me ( v Telephone( ) . ----'---'=·_:,_I'_________ _ _ __, ______ _ Adciress S f ei J e "? v i'J / t. Collector's Name ~, "?~ signature Date S=pled /CJ la LJ le 'y : ' ✓ ' Tele_phone('J/ "/ ) 7 .S 3 -~ 8' () ( Ti.me Sampled _ ____,/_4..,__;;;_0=...,0,:,_ ___ _ Type of Process Gene~2 ting Was te __ -+,f~c_·· __ .,,_/_/_c_· _;_c/_e_._S_·· _______________ _ '-tc .&;-? Chain c: Possession: 1. k~ IO/i'f-10/2s !1tf signature title inclusive· dates ···-. 2. signature "r, i-c.-in-. 1 ~ ,,.._f) · ('/.,v'1,/'~gc~~Z7· /.::? ;_..:?S~-f/· title l --'-:in---'cC::1-u_s.sic.:v:.s.e_d_a_t_e_s __ 3. signature title inclusive daces Res~:::s reported signature tir.le dz:e lns:::-uc~ions: Complete 2.11 applicable infcn:.ation incluciing sign2tures, and submit: ~it:h ·2nalysis .eques: fo=s. • • STATE LABORATORY OF PUBLIC HEALTH -• . DIVISION OF HEALTH SERVICES, N.C. OEPARTHENT OF HUHAN RESOURCES PO eox 28047 306 N WILHINGTON ST RALEIGH NC 27611 ORGANIC CHEHICAL ANALYSIS Date bf Analysis Lab No. C,ll/:J IA{//} Q/','110/ PURGEABLE COMPOUNDS HDL Field# -Tv= c I 1 ( I 1 __ ,,_,.,_ ·•-,i"--A'in/11 .. n/On /41f l -"·- Dichlorodifluoranethane A n t. I Chlorcmethane I {Vinvl Chloride erooonethane -Ch 1 oroethane , Trichlorofluoranethane I ✓l. 1-0ichloroethvlene lL lf Hethvlene Chloride I tert-Butvl Hethvl Ether -__ (Trans) 1 2-0ichloroethvlene Ism~ul ether -I_. 1-0ichloroethane ~ 111 . 2 2-Dichlo ne l I (Cis) 1.2-Dichloroethvlene I, l11 - Chlorofonn /, '7_ ..,. _ _(8CH) 8raoochloranethane " ✓I I. I-Trichloroethane A, " I 1-Dichlo, ne u.... {Garbon Tetrachloride I K {Benzene I - ✓I 2-Dichloroethane IJ!.. {.l rich loroethvlene -,; _ 1.2-Dichlor --·ne I ermodichloranethane Dibrooonethane Toluene -' .. 1 1 2-Trichloroethane I -Tetrachloroethene /.. ,;i q_ -1 3-0ichlo ne ... Dibrarochloranethane ___ l,2 Dibronoethane (EDB! ! 1--Chlorohexane \!/ 'JI ·-· -~ -- -----·· ----· CONl'ENTS: J .. Estimated value. K .. Actual value is kllOl-!n to be less than value given. L -Actual value is known to be greater than value given. U -Haterial was analyzed for but not detected. NA .. Not analyzed. 1/ -Tentative identification. HUL -Minilll.fll Detection Limit for water (EPA Hethod 5D2.2), µg/1. ✓ --He9ulated voe T .. Tri ha lcmethane N.C. Division of Health Services OHS 3068-0 (4/88 Laboratory) ', , I /.tn I I ·/ I< ( 1 ( ) ··-/1 ---"•-. -'1 . /l,,. --------- .. .. ;n/21_!;; I , ( ) ,n/] .. n/Cn • STATE LABORATORY Of PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. DEPARTl1ENT Of H\J!IAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON ST, RALEIGH, N.C. 21611 ORGANIC (ljEMICAL ANALYSIS Lab No. x.n ,,,,/ F.I~) PURGEABLE COMPOUNDS MDL Field# -T= ( /. l ~~="m • •--.i '---.,,..,-;---,a1 ,.,,..JL,,.. Ch lorobenzene I Ai'lh II Ethvlbenzene IV I · 1 l. 1.2-Tetrachloroethane D-Xvlene m-Xvlene o-Xvlene Stvrene Braoofonn I lbenzene l l 2 2-Tetrachloroethane Braoobenzene n-P~ulbenzene -1.2.3-Trlchlo, -ne -2-Chlorotoluene -1.3.5-Trirrethvlbenzene . 4-Chlorotoluene (Tertl Butvl Benzene Pentachloroethane 1.2.4-Trirrethvlbenzene :<sec) Butvl Benzene R-Is ltoluene l 3-Dichlorobenzene ✓1.4-Dichlorobenzene n-8utvlbenzene l 2-Dichlorobenzene (Bis) 2 Chloroi 1 Ether -· _J...2-Dibraoo-3 Chlo ne _ h_2.4-Trichlorobenzene Hexachlorobutadiene Nanhthalene -_ l,_2.3-Trichlorobenzene \I/ \ I I -· ---· J -Estimated value. K -Actual value is known to be less than value given. L -Actual value is kno;,n to be greater than value given. u -Material was analyzed for but not detected. NA -Not analyzed. 1/ -Tentative identification. MDL -Minimum Detection Limit for water (EPA Method 502.2), µg/1. ✓ -Re9ulated voe l -Tr1halorrethane N.C. Division of Health Services OHS 3068-0 (4/88 Laboratory) 9n'Jt_ SI ( /) l.-'"- , ,/ ( ) • ,,.,, ..... JL, ... ---- ( ) ( ) , ,,.fl 111'1/L-n un/J un/•n BASE/NEUTRAL AND ACID EXTRACTABLES rotlPOUND N-nitrosodimethvlamine bi s<2-ch loroethvl lether 2-ch l orooheno l ohenol l 3-dichlorobenzene 1.4-dichlorobenzene 1.2-dichlorobenzene • STATE LABORATORY Of PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES P.O. BOX 28047 -306 N. WILHINGTOO, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS LAB NO Yl/l2,ui'l<J ,< 0 ? I _.l"/S FIELD # L//00 t..J/ 0 ?.- TYPE l I l < I \ ( l ( l UNITS r.;n/] ,.,,,.,,,., · .. n/ l ),m&l ""' l .. n/ko o,n/ l .. n/ko 10/_::/3() ~ (,,L bis(2-chloroi llether hexachloroethane N-ni troso-di-n lami ne nitrobenzene 1<-rv">horone 2-n i trooheno l 2 4-dimethvlnhenol bis(2-chloroethox"'methane 2 4-dichloroohenol 1,2 4-trichlorobenzene nanhthalene hexachlorobutadiene 4-chloro-m-cresol hexachlorocvcl~ntadiene 2.4.6-trichlo~henol 2-chloronanhthalene acen>nhthvlene dimethvl ohthalate 2 6-dinitrotoluene acenanhthene 2 4-dinit~henol 2 4-dinitrotoluene 4-nitroohenol fluorene 4-chloroohenvlohenvlether diethvl ohthalate 4.6-di ni tro-o-cresol diohenvlamine azobenzeoe 4-o=henvlohenvlether hexachlorobenzene =ntachloroohenol ohenanthrene anthracene dibutvl ohthalate fl uoranthene , SOh0-'iO u,l330 ,:-0/,1 • .::0 10/_g30 J, so, ir,,,n J,, Ir, 1..330 ,,.,,~_,n s-01✓1.so ,.,, / ;/30 ,, ffi"])L H,.o/so11-- ' I J -Estimated value. K -Actual value is known to be less than value given. •7 ( l ,on/ l .. n/ko L -Actual value is known to be greater than value given. U -llaterial was analyzed for but not detected. The nurrber NA -Not analyzed. is the 11ininun Detection Limit. mI>L --- 1/ -Tentative identification. ~I -On NROC List of Priority Pollutants. N. C. 0-i.v.w-i.on 06 He.aLth SVtv-i.c.v., OHS 3068-0 (4/86 LaboJta-to~y) - ( ) ,on/1 uo/kq e STATE LABOMlOHY Of PUBLIC HEALlH DIVISION Of HEALlll SERVICES, N.C. OEPARlMENl Of HUMAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON, Sl., RALEIGH, N.C. 27611 ORGANIC °"EHICAL ANALYSIS BASE/NEUTRAL ANO AC!O LAB NO l'<O.., /Af-1<-/ x'O -,,_ o.r- EXTRACT ABLES FIELD# '-I I 11 n l.f/02- aJMPOONO TYPE ( I ) ( I l ( . l ( ) UNITS (µo/ li uo/ko /uo/ 1) ua/kq ua/1 uo/kq .. n/ 1 .. n/ko ovrene /0/.•'iO iL-IL benzid\ne ,...~ /,t,50 butvl benzvl ohthalate 101:130 benz(a)anthracene chrvsene . 3 3-<lichlorobenzidine so/11-,-'i'll bi s(2-ethvl hexvl )ohtha 1 ate llo/330 di-n-0etvl ohthalate IO/.J.~o benzo(b)fluoranthene So /t t,,;n benzo(klfluoranthene benzo(a)ovrene indeno(l .2 3-cdlnvrene dibenzo(a hlanthracene benzo(q .h. i \o,,rvlene ' I ,J ,/ ani 11 ne l<o' -~ fA_.. \).... benzoic acid I benzvl alcohol ,/1 4-chloroani 1i ne ir.1-.:,,0 dibenzofuran 2--methvl=nhthalene 2--methvl oheno 1 4--methv 1 oheoo 1 ,J,. 2-nitroani 1 ine s-01,1,.,.0 3-nltroani line 4-ni troani line 2 4 5-trichloroohenol ,,. '.-' / mnL J -Estimated value. H:z.0/ Soll-. K -Actual value is kno«n to be less than value given. L -Actual value is kno«n to be greater than value given. U -tlaterial was analyzed for but not detected. The nunoer is the Hininun Detection Limit. NA -Not analyzed. 1/ -Tentative identification. ~I -On NROC List of Priority Pollutants. N. C. 0-<.v,U.,-<.Otl o 6 He.aU/i SVtv-<.c.<!./2 VHS 3068-0 (4/86 Labonn;to~y) ( ) ( ) oon/ 1 oon/ka uo/1 110/ m:in .. - 26 July 1988 TO: File FROM: Grover Nicholson RE: Trip to FCX-Statesville On 21 July 1988 I met with Don Rigger of the Emergency Response and Control Section, US EPA, 404-347-3931 and with Cody Jackson of ATSDR, EPA Region IV. We met at the FCX site in Statesville and reviewed the soil and groundwater sampling previously done, discussed the probable location of the buried DDT, and discussed the groundwater use in the surrounding area. The purpose of the visit to the site is to help Rigger and Jackson determine if it is appropriate and feasible to remove the buried DDT. Primarily, they must decide if contaminants found in the groundwater are moving from the buried chemicals or from general soil contamination resulting from daily repackaging of pesticides. Secondly, they must decide if there are sufficient groundwater targets in the area to warrant a removal. GN/ds/grover.58 TO: FROM: RE: File Grover Nicholson FCX-Statesville Site visit to site with EPA - 19 July 1988 I telephoned the Iredell County Health Department (704-873-7291) today and talked with Margaret Burke, environmental secretary. I left a message for Kelly Sheeks, Environmental Health Coordinator, that an EPA representative and I would be at the FCX facility in Statesville on Thursday. Ms. Burke said that Mr. Sheeks would probably call back and that he would notify the county health director. GN/ds/grover. 55 -- North Carolina Department of Human Resources Division of Health Services P.O. Box 2091 • Raleigh, North Carolina 27602-2091 James G. Martin, Governor David T. Flaherty, Secretary Ronald H. Levine, M.D., M.P.H. Ms. Susan Deihl EPA Region Waste Division EPA NC CERCLA Project Officer 345 Courtland St., N.E. Atlanta, GA 30365 Dear Ms. Deihl : RE: FCX-Statesville 28 June 1988 Eyewitness account of waste disposal State Health Director As per our conversation, I am sending a memo to file about my telecon with Mr. Phil Keller, an eyewitness to the disposal at the site. This information may be of help during remediation. Please add it to the FCX-Statesville SI file. GN/pb/grover.39 cc: Ned Jessup, OSC Kim Dao, Cost Recovery Sincerely, l-::-:holsoo, Goologisl Superfund Branch Solid Waste Management Section ----- 24 June 1988 TO: FROM: File Grover Nicholson 9-,~ ;(/~1 ,,___ RE: Eyewitness account of waste disposal at FCX-Statesville. I received a call today from Phil Keller, Probation and Parole Department, 301 Davie Avenue, Statesville, NC 28677, (704) 873-4391. Mr. Keller worked for P.S. West Construction Company of Statesville during the summer of 1969 as a laborer. (He was 18 or 19 years old.) For three days he worked on the construction of the addition to the FCX facility on Front street in Statesville. During those three days he witnessed and helped with the disposal of waste chemicals at the construction site. Mr. Keller reports that SO-pound bags and I-quart glass bottles containing chemicals (he thinks DDT and Chlordane) were thrown into a low area prior to the site beginning backfilled and before the concrete floor was poured. The bags and bottles broke or did not break depending on how they fell. The building site was lower than the existing building and up to 8 or 9 feet of fill was placed before the floor was poured. Mr. Keller remembers the disposal location as being almost in the center of the building where the addition joins the old building. Mr. Keller called after reading about the site in the Statesville newspaper. He agreed to be available to help locate the disposal area, if necessary. GN/pb/ grover.35 - TO: File FROM: RE: Grover Nicholson FCX-Statesville - 24 June 1988 Susan Deihl called and reported that Larry Snoddy of Rubbermaid in Statesville, (704) 878-9551, called Region IV US EPA. He reported that Rubbermaid now leases part of the FCX facility in Statesville and employs up to 8 people, 3 shifts per day, 40 hours per week, to package potting soil in one-cubic yard containers. After reading the newspaper article about FCX, Mr. Snoddy was concerned that his employees might be exposed to pesticides. Susan wanted us to be aware of the potential problem and was trying to find out if any EPA program could sample the air in the work area. I called Bill Williams in the Pesticide Program, 733-3410, and explained that situation. He said that either the Pesticide Program and Occupational Health Branch would do air sample in that situation. Bill said that both programs routinely offer that service. I relayed the information from Bill Williams to Susan Deihl. GN/pb/grover .34 -- 23 June 1988 TO: File FROM: Grover Nicholson f-/..),:...,f___ / .,,-.-- RE: FCX-Statesville Contact with concerned citizen. 1 spoke via telephone today with Ellen O'Brien of Statesville, NC. Her address and telephone number are: Rt. 2, Box 229, Statesville, NC, 28677, (704) 632-2136. She is associated with the Clean Water Fund and with the Blue Ridge Environmental Defense League. She want to know details included in the FCX-Statesville SI -what sampling had been done, what contaminants were present, etc. After I gave here some information, I suggested that she make an appointment to review the file or contact US EPA FOlA officer for a copy. I gave her Region IV's address and telephone number and sent her a copy of Wastlan and FOIA information. GN/pb/ grover. 36 Form No. 1034 Rev. 6/88 North Carolina Department of Transportation REPRODUCTION WORKORDER-HIGHWAY PRINT SHOP Date Projec.t No. Order No. _______ _ TYPE OF REPRODUCTION PHOTOCOPY: D Xerox9400 OFFSET: 0 Multilith r2so WET: D Ammonia /) /4'!:...o. Dept. No. M;~,;,; r..1// Phone No. ·:; 5] -? [';{) I ·? t·-, -pr 0 / / Room Np.-: -·· j _::.: c-, r_.· ... /~L--=-( jJ j ,·· / Auth. -~1-: c.·-.....--~-,v· ..--~ .. ~ ,.....,...,___.. I !. □ Xerox 7080 D Multilith 1850 0 Mirco-Film SIGNATURE / (Ji!I-XBro X 2080 D Xerox 9900 Masters, Forms, Z-/ Front & ~nt Tracings, etc.--~~--No. of Copies _____ D Back C::1> Only (NUMBER SIDES) COPY SIZE: Sheets D 8½X11 D 8½X14 D 12X19 0 24X36 D Other Rolls D 18X --)<: 24X C'7 D 36X __ D 42X _ □ Other ,/1/'. PAPER: _pu-J:'lain D Bond D Onion D Color D Letterhead lJ Blu·e-line D Sepia O Vellum INKS: D Red D Yellow D Green D Blue i)2hlllack 0 Violet □· Other _______________ _ . HANDLING: D Collate □ C/S D Normal D Punch D Cut D Rush D Staple, D Fold □ C/P/S D C/F D C/P D Bind Special Instructions: ,., , . _ ( = .£/ ~ lf-;o /Jr <h' (\ .. ., I F// ' . r ;~:-✓v~C--1 L::..{ 5(-S' h& v-:l(I? fh..1.Li a.,'1 (c s-f O !i(£Q... ,. /-':) 1-::> )4 -/, --c· ( ·, ,-;i ; i/71 / f/ ::::-,, , I Jf...•V /'Jt':,,-\ ,)d/Fl{,tYC _;;;,CC7" ~ . -( :(-' I f I ·-~ i TO: FRCM: SUBJECT: 10 May 1988 File Jack Butler Telepmne ronversati.Dn with Stewart Hodges, FCX (919-828-4411) aoout FCX Washington, OCD98147 5932, and FCX Statesville, N::0095458527 Mr. Hodges rep;:irted that 3 acres of the FCX Washington property including the waremuse had been sold. Bags, bottles, jars, etc. from the waremuse and grounds was drumed and renoved as hazarc:bus waste by GSX. 1he bags, jugs, etc. in the on-site landfill have not been disturbed. There are no monitoring wells on the site and an on-site drinking water well was closed and capped in 1985. Mr. Hodges rep;:irted that there has been no clean up of pesticides under the waremuse in Statesville and no new monitoring wells. JB/ ds/05 72b .65 -- North Carolina Department of Human Resources Division of Health Services P.O. Box 2091 • Raleigh, North Carolina 27602-2091 James G. Martin, Governor David T. Flaherty, Secretary Ronald H. Levine, M.D., M.P.H. 4 May 1988 'IO: Nancy Scott, Associate Attorney General Attorney General's Office FROM: William L. Meyer, Chief Solid Waste .Management Section RE: Immediate Action at FCX Washington ard FCX Statesville State Health Director 'Ihe State should request that FCX install rronitoring wells at facilities located in Washington ard Statesville immediately to determine whether or not groundwater contamination is migrating beyond the property boundaries. If you have any further questions, please contact rre at 733-2178. WIM/tb/a-10 North Carolina Department of Human Resources Division of Health Services P.O. Box 2091 • Raleigh, North Carolina 27602-2091 James G. Martin, Governor David T. Flaherty, Secretary Ronald H. Levine, M.D., M.P.H. Ms. Irene Kiefer WH548-A US EPA 401 M. Street, SW Washington OC 20460 Dear Ms. Kiefer: State Health Director 31 December 1987 SUBJECT: Legal status and present a..mership of FCX-Statesville, NCD095458527, and E'CX-Washington, NCD981475932. E'CX, Incorporated filed for bankruptcy under Chapter Eleven and began a complete liquidation of assets on 16 September 1985. The present FCX contact is J. Stewart Hodges, V.P. FCX, E'inancial Administrator, 609 St. Marys Street, Raleigh, NC 27602, (919) 832-6047. He supplied the following information. The FCX facility in Statesville, NC, land and buildings, is still a-med by FCX, Inc., Debtor and Debtor-in,-Possession. Space in the warehouse is being leased, 30 days at a time, to Rubbernaid for raw naterial storage. There is no contamination study or remedial action in progress at the site. Ms. Irene Kiefer 31 December 1987 Page 2 -.. The FCX facility in Washington, NC was sold in two parcels and no part of the site is presently o..med by FCX, Inc. In August 1986, Fred Webb, Inc. of Greenville, NC bought the nain warehouse and four acres of land. The pesticide burial trench is =ntained on this four acre parcel. In August 1987 the renaining two acres containing a block building and another small building were sold to W.B. Gerard and Sons, a fertilizer distributor next door to the FCX facility. There has been no additional site study or remedial action at the facility since the site inspections by the NC CERCIA Unit in August and November 1986. Previously, GSX, Inc. had cleaned the block building, which was used for chemical storage, and had investigated the contamination in the trench area. Tne warehouse was not cleaned. If I can be of further help or if you have any questions =ncerning this information, please call me at (919) 733-2801. GN/pb/0479b.82 Sincerely, CJ,~ )J;,,,tcf- VGrover Nicholson, Geclogist CERCIA Unit Solid and Hazardous Waste Management Branch Environmental Health Section Form No. 1034 Rev. 9/85 - North Carolina Department of Transportation REPRODUCTION WORKORDER-HIGHWAY PRINT SHOP Date 21 J t/,Ut 3' 1-Dept No. r-/4ma&1 ~- Project No. Order No. ______ _ TYPE OF REPRODUCTION PHOTOCOPY: □ Xerox 9400 OFFSET: WET: □ Mullililh 1250 D Ammonia Phone No._~:.:j_7~:1_-~(~g'~0~/ __ □ Xerox 840 □ Multilith 1850 D Mirco-Film ... · ~erox2080 Masters: Forms, / / Front & ~Front Tracings,etc. ___ ~_No.ofCopies __ ~-□ Back Only (NUMBER SIDES) COPY SIZE: Sheets □ 8½X11 □ 8½X14 □ 12X19 □ 24X36 □ Other Rolls □ 18X_ □,A4xA □ 36X_ □ 42X_ □ Other PAPER: l>(P1ain □ Bond □ Onion □ Color □ Letterhead IJ Blue-line □ Sepia D Vellum INKS: /)<§tack □ Red □ Yellow □ Green □ Blue □ Violet □ Other HANDLING: □ Normal □ Rush □ Collate □ Punch □ Staple □ CIPIS □ C/P □ CIS □ Cut □ Fold □ CIF □ Bind Special Instructions: ---.----------,------- ?Udt a:,;l -L/XJ Jo 7v:,y 'if'r- 7 I • Form No. 1034 Rev. 9/85 • North Carolina Department of Transportation REPRODUCTION WORKORDER-HIGHWAY PRINT SHOP Project No. Order No. ______ _ TYPE OF REPRODUCTION PHOTOCOPY: □ Xerox 9400 OFFSET: □ Multilith 1250 WET: □ Ammonia Dept. No. llt/,'1,4/U /2.ES Phone No. "f:5"g -Z't () I Room No. Z/'3 'B:EH~ Auth. ~ sTGf':ruRE I □ Xerox 7080 Merox 2080 ,Y:·"fvellum) □ Multilith 1850 0 Mirco·Film A Masters, Forms, Z J ~ront & ~ont Tracings, etc.· No. of Copies (c □ Back 'I' .nly (NUMBER SIDES) , COPY SIZE: Sheets □ 81/,X11 Rolls □ 18X □ 81/,X14 □ 12X19 □ 24X36 □ Other }(24X~ □ 36X_ □ 42X_ 0 Other PAPER: }<:Plain □ Bond lJ Blue·line □ Sepia INKS: ~I -:Black □ Red \ D Violet D 01her HANDLING D Collate D C/S D Normal D Punch D Cut □ Onion D Vellum □ Yellow D Rush D Staple D Fold Special Instructions: L WA _a,' -'1/2 I □ Color □ Green D CIPIS D C/F □ Letterhead D Blue D C/P D Bind -f-Zl-'i?'r Form No. 1034 •·· ·· h Rev.9/85 U Nori arolina Department of Transportation REPRODUCTION WORKORDER-HIGHWAY PRINT SHOP Project No. Order No. ______ _ TYPE OF REPRODUCTION PHOTOCOPY: D Xerox 9400 OFFSET WET: 0 Multilith 1250 0 Ammonia Dept No. //4.,~a<c k,1,,u,ccµ Phone No. :7 J: ?-?-Zc, I RoomNo. l?'Y 8c,-fi:_ Auth. (,::/,,....,,_ D Xerox 7080 0 Mult1lith 1850 D Mirco-Film SIGNATURE D Xerox 2080 (Vellum) Masters, Forms, / 7 Front & Tracings. etc.--~-No. of Copies __ ,__ __ D Back i.J.. Fron! 7 ,only COPY SIZE Sheets Rolls PAPER: INKS: (NUMBER SIDES) 0 B½Xi 1 D 81i,X14 0 12X19 0 24X36 D Other cy;4x 21 O 36X_ O 42X_ o OIiier 0 Bond 0 Onion 0 Color □ Letterhead L1 Blue•line D Sepia O Vellum rXs1ack O Red O Yellow D Green □ Blue 0 Violet O Other _______________ _ HANDLING 0 Normal D Rush D Collate □ Pun~h D Staple D CIPIS 0 CIP D C/S 0 Cul □ Fold D C/F D Bind Special Instructions: f{,/,I( /}/v/r v[> 1-/1-ft I I • . _._SUDDIN SIIVICI: ., ,__.____,, RALEIGH BLUE PRINTEl(S Blue Line Prints, Intermediates, Engineering Supplies Maps (Agents tor U.S.G.S. Maps and Nautical Charts) 313 W. Martin Street• Raleigh, North Carolina 27601 • (919) 832-2841 cusrnMER Gr2ove ic N ,c 1-1 oL-sr:, , .. J ADDRESS 2wv,,c.ol,,J. 1-IEnc:TH 5"cc.:'-::,,: .. .! R rf\ z..o 3 ~AI H f I -'l:::6 f, -rr L✓ . - ~ .. ,,. . r.--. ' /,,.., -.. ( 1, , C7 ~;~,. : .... FC..Y -:,-1,.;t,.. ,;,!/ <.--/2,(,,D F LJ -w..,, /,:, , < 1-r,.,.. -(. , t D _,, ..... I , , . ,-,-:, .,. /) 4 I j -f. L-,,p-; ~ / v lc.,,r,·~1 S·"'__... ; / ' DELIVER □ fllrt,\C'-' , i\\\'; AL . , PICKUP □ 1,_1:,,4, ~ 'fl\'.). "?i\'\ t.~ s □ 'i'>-'-t,.S· ,, ·\.'\ t;ii'-1 TAX MAIL \,\()\•\'' \l,i'-\\_t.l>• ~\) \',t. TRANS. TRACING RETURNED □ 3810 TOTAL CUSTOMER /~ ·CJ 0 , C)() , /d· ?0 ' \ 1/ POTENTIAL HAZARDOUS WASTE SITE L IDENTIFICATION 8EPA 01 STATI; 102 SITE NUMBER SITE INSPECTION REPORT /.IC Do 9.,1/., Rs 2 7 PART 1 • SITE LOCATION AND INSPECTION INFORMATION I~ SITE NAME AND LOCATION 01 S:TE. hA.ME ,~.COITVflOll,OtOHC:,.,,,__., .. ., 02 STREET, ROUTE NO., OR SPECIFIC LOCATION &OENTIAER Fcx .s 1,,£,,J.(),, IC 2-o u/__,,,f h-, 0V, j _.;/£,,,, . ./ . 03 C:ITY CM STA.TE OSZIPCOOE 06COUNTY 07COUNT OOCONG Jf ~/4 C00E 01ST ;Ve. ::1-gi,, ·;-7 -:f',,,~/1. jJ I'. ~9 9 Oil CO<OfiOlNATES I 10 TYPE OF OWNERSHIP {CIIKt _, LATTT\JDE LONGmJDE l!l' A. PRIVATE □ B. FEDERAL □ C. STATE OD. COUl<TY OE. MUNICl?AL 3S .!f.2 ,Pf:.. /( I) .<., I 0 0 □ F.OTHER □G.UNKNOWN Ill. INSPECTION INFORMATION 01 ;:IATEOFINSP~;TtON 02 SITE STATUS 03 YEARS OF OPERATIOH S, 71 ,ii(. D ACTIVE ~ I 9'f'o I /CJh'f _UNKNOWN M0,"1TH. DAY YE"-" ll'J'INACTIVE BEGINNING YEAR ENDING YEAR :.c. A.G.::NCY P~Rf0RMING tNSPECTION r.:::r-,t:,. _, .-,,J 0 A.EPA □ B. EPA CONTRACTOR· 0 C. MUNICIPAL □ D. MUNICIPAL CONTRACTOR ,_,,_ _,..,..., %E.STATE 0 F. STATE CONTRACTOR □G.OTHER ,,,_;,i;;.; (So•ptyJ t.,~ C.,1:;:;: lN5PECTOR 06l1Tl.E 07 ORGANIZATION 08 TELEPKONE NO. 1-1 tVv.-, LL,, 4':d',._,,, -~,m,, ~'" l~t f'./1.,.,.;, ,1 /JH., l..wuf ( 91,I 7.$-r-z JOI VS OTHER l~E:CTORS 0 10 lTT1.E 11 ORGANIZATION 12 TElEPHONE NO. A~-n,-,..J )u~a-C.,.,,,,,.; __,/,1, ,-/J,,, ., ;,__, -I /I ( ) . ~c ;1,-£1b, . (/ ( ) . ( ) ( ) l ( ) \ ~ f.lTE AEP'~ESENT ATIVES INTEA'/11:WEI) 14 lTTl.E 15ADORESS 1 & TELEPHONE NO ~-·{6 ,I t-/-" -Fc.X l7oy> f72-S~/ .,.._, fl . 11/Ll,,o a iu,J -✓ ' ?o C,./l_ P~.1 ~flt~f })AAA/,,_, AJc. 1'119) 'r£?-/Rti '1, , ( ) .. ( .) ( ) . ( ) .. l □;';:::.';_".~ BY 16 TIME OF t<SPECTION 18 WE4THER CONDlllONS PEAMl~ON ,.,,, C&w /nurJ,_,af.L -f. 6~~ ~:~,..;70d,,, _w.,RRAflf 1:' 0 -1 ';/ ':) ·- 1 IV. l!IFORilATION AVAILABLE FROM . ~--020FfA~,IOrpa,'IU:__, 03 TEl.E.PHONi= NO. I ~1 CO~"'TACT l~.!~Pa,,f ~~~!.£ FCX lc/19 I J?Jz -t,o,f7 l ~ ... 1->f.W.,):• f.':!;SPONSI..L.E.F&iA'E 1,-.SPE FORM 05 AGENCY 0e OAGA.NIZATtON 07 TELEPHONE NO. 08 Oo\Tc (919) ;-~3-.:i~o/ 7 1-'5£ )i'(,. U(~<fel',._ ljJ n1';-£,,L,,,.,.., ,Ve nµR /4/Js: S/f«J J11..,_.,,/ &. ~ DAV ''t'EAI' , POTENTIAL HAZARDOUS WASTE SITE L IDENTIFICATION &EPA SITE INSPECTION REPORT 01 STA.TEI 02 SITE HUMBER PART 2 •WI-STE INFORMATION #C. r, O"i<",;,.,,-RS2. 7 II. WASTE STATES, QUANTITIES, AND CHARACTERISTICS 01 PHYSICAi.. ST,.TES 10-a .. _,_,.,,,., 02 WASTE.QUANTITY AT SITE 03 WA.STECHA.RACTe:RlSTICS ,c,_. .. .,._,..,, , ... _,., _.,. ..,._., J1!._A.. TOXIC ,!!!•-souo ~-SLURRY -.i --Jl,eftCIIMU CJ E. SOI.IJIILE CJ I. HIGHLY \'Ou.'111.E □ B. POWDER, FINES . UOUIO TONS t, f 3~ 5 0 B. CORROSIVE 0 F. INf:ECTlOIJS 0 J.EXPLOSlVE C C.S.UOGE CJ G. GAS 0 C. RADIOACTIVE 0 G. Fl.AMMASL.E C K. REA.CTIVE CUSICYAROS }( D. PERSISTENT 0 H. IGNITABLE □ L NCOMPA.TlBLE 0 C.OTHER □ M. NOT APPUCABLE ,~,, NO.OF DRUMS Ill. WASTE TYPE CATEGORY SUBSTANCE NAME 01 GROSS AMOUNT 02 UNIT OF MEASURE 03COMMENTS SI.U SI.UDGE OLW OILYWASTE SOL SOLVENTS (PSO) PESTICIDES 7-/tJoou Pa-d', FC,< /,.. ~ ..I tJ A ITV> , ~ .tv _A occ OTHER ORGANIC CHEMICALS 11.1.,,,,,./,; :r-1,,, -~ -_,,,; 'ry, J V IOC INORGANIC CHEMICALS /I ACO ACIDS BAS BASES MES HEAVY METALS IV. HAZARDOUS SUBSTANCES (SH~._.,,,_,.,.,,,. dr,d CAS ,,,..,,..,., 01 CATEGORY 02SUBSTANCE~E 03 CAS NUMBER 04STORAGE/tMSPOSALMETHOD 05 CONCENTRATION 06 MEASURE Of CONCEN'TRA.TlON PS.D Dt>T (l . ,,,...,,1..,,,. •• J / Jfo.'//,,., .N/4 p51) -{,_. ,I"""-' f/ • • ,, " ... i:,<"t,_ . -. f _fl Ln .L ____._ I/ ,, Psn F),',_ P,.t,_,:_, __ ,, ,, PSD r..U -II -I/ V. FEEOSTOqKS (S..""'91'0r•lotCA.$H_,_., CATEGORY 01 FEEDSTOCK NAME 02 CAS N~MBER CATEGORY 01 FEEDSTOCK NAME 02 CAS NUMBER FOS I FOS FOS I FOS FOS I FDS FOS I FOS VI. SOURCES OF INFORMATION ,c ... .,,,.,.11:,.1•-••· '·"··"•••,..•·,-oi..,..,f.,.,,_,,., __,£t_ ~, ~ _ ;_ -~ -? -;,.,°?f I 7 g 6 i p ~.....:, ~ c:~t . ~ ~ .);.,,-,,...1 I 9 f e, I EPA FORM 2070-13 (7-81 I • POTENTIAL HAZARDOUS WASTE SITE L IDENTIFICATION &EPA SITE INSPECTION REPORT 01 STATE l 02 &l1'E NUMBER PART 3 • DESCRIPTION OF HAZARDOUS CONDITIONS AND INCIDENTS Al c... I\ 0 q, S 'I ~.P< 2 7 ' IL HAZARDOUS CONOmONS AND INCIDENTS 01 )il'. A. GROUNDWATER CONTAMINATION . . . _ 02,Ji1 OBSERVED iOATE: 7 ;;,., 1f.P." I □ POTENllAI. □ AI.LEGED OJPOPULATIONPOTE~TIAllYAFF~CTEO: /'',(;,':, . 04iNARRATIVEOESCRIPTION " · .. o-J ~. I, .;p , .. /'· tP ra,I,._, J<> 1 _,_.,, _,;t;-.....-, ~~ ~; //I ,,,,._,,.. ~ I ~ ~ S-,,,.:,__e, /I adc,;__, I ·-.. I 01 0 8. SURFACE WATER CONTAMINATION of□ OBSERVED IOATE: l 0 POTEh'l\AI. D A1.LEGED 03 POPULATION POTENTIAll Y AFFECTED: 04 I NARRATIVE DESCRIPTION IM'~ ' -,{} /_. I I 01 0 C. CONTAMINATION OF AIR . 02: 0 OBSERVED IDA TE: l D POTENllAI. 0 ALLEGED 03 POPULATION POTENTIAll Y AFFECTED: 04, N,ARRATIVE DESCRIPTION )./L i .. I 01 D 0. FIRE/EXPlOSIVE CONOmONS 02: 0 OBSERVED IDA TE: l D POTEtffiAL 0 AIJ.EGEII 03 POPULATION POTENTIALI. Y AFFECTED: 04 1 NARRATIVE DESCRIPTION .. ;f/l ' I ,., ' I ,:_ __ , -. ·o,-~e: DIRECT CONTACT · 02 D OBSERVED IDATE: l /1f POTENllAI. 0 AI.LEGED 03 .POPULATION POTENTIAll Y AFFECTED: S<f ,-'( ii-;..,· 1/,J, 04' NARRATIVE DESCRIPTION I '' --~a-,/c,.<-4/ ,-<,<.1..,a.f =~~--~ ~ __;___,,,,,_d ~ --¾ r~ - ./)V t,,,,,.,_e -s dcv-e ,,_IJ.,,..,,_;f /a,n Hof,.,-/,-'--<.. ~tf ~. lat a,,.£"4-,,,,_,a.J.a.' 01 )ll F. CONTAMINATION OF SOIL .5 O~}.!i;OBSERVEOIOATE: •7m;y /9..176) D POTENllAI. 0 AI.LEGED 03 AREA POTENTIAll Y AFFECTED: 04. NARRATIVE DESCRIPTION /?& f,'c , ,I -0 .-cf, . · IACfNI , ·C,c-,J! .,.,_, d,;,/J(,,li::.. ~ J ~ ~ ,0~-4,.,- ! ~~ G. DRINKING WATER CONTAMINATION / 3/,,,; . 02· D OBSERVED IDA TE: l ~TEtffiAL □ AU.EGEII 0 OPULA TION POTENTIALI. Y AFFECTED: , · 04'NARRATIVE DESCRIPTION J-f ~ /,,__..._.;._.c,,/, -.,._ ~ad~ ,..,_,.,,_, i ti'(;" ·f, ' ' I 01 -re. H. WORKER EXPOSURE/INJURY 02 0 OBSERVED !DATE: l ;lfl POTEtffiAL 0 AIJ.EGED 03 ORKERS POTENTIALI. Y AFFECTED: -04' NARRA TlVE DESCRIPTION .,,Le.~a-l~-1- I -.. I -. • : - ' I ~~I.POPULATION EXPOSURE/INJURY 02 0 OBSERVED IDA TE: l pf POTEtffiAL. D AU.EGEi) O POPULATION POTENTIAUY AFFECTED: 04, NARR A TlVE DESCRIPTION I ~ ~ ,/4-l-~a,}'-1f,=c( ~r,,--, ~&,..,;.:..J ,oa.,t;. I I ,SEPA POTENTIAL HAZARDOUS WASTE SITE SITE INSPECTION REPORT L IDENTIFICATION 01 STATEl02 srTE NUMBER PART 3 • DESCRIPTION OF HAZARDOUS CONDITIONS ANO INCIDENTS 111 '-I fl O 9 <''1',R <;2. 7 IL HAZARDOUS CONDmONS AND INCIDENTS ,_, 01 □ J. DAMAGE TO FLORA 04 NARRATIVE DESCRIPTION l{!L 01 C: K. DAMAGE TO FAUNA 04 N.'RRATIVE DESCRIPTION 1#t(w.,-.,1101apeeM1J 01 □ L co~ ,.Mll<'-TION OF FOOD CHAIN 04 NARRATIVE DESCRIPTION AIL ' 02 t;) OBSERVED IDATE: _____ ) 02 t;) OBSERVED !DATE: _____ ) 02 0 OBSERVED (DATE: _____ ) ! 01 Jlil' M. UNSTABLE CONTAINMENT OF WASTES 02 0 OBSERVED !DATE: _____ ) 1~•Aut>o,1:_•s,•,_11~L.Hb!Qo,_) ,.., / I 03 POPULATION POTENTIALL V AFFECTED· ~,rwvv 04 NARRATIVE DESCRIPTION □ POTENTlAL □ ALLEGED □ POTENTIAL □ ALLEGED 0 POTENTlAL · □ ALLEGED .Q(POTENTIAL 0 ALLEGED ~ -J 1 A.-Vtu2./4_-..;,,, ~~,j..J._, 1_..-u., f :,,,,~I ~ ,-,,,,,....c.;..<:,_ --tJ ee,.Jbl'~t,.. A.AJC</J/.JJ /~ ....,._J ~ f. _ ,-1....__. I 01 C N. DAMAGE TO OFFSITE PROPERTY 04 NARRA 'flVE DESCRIPTION 02 0 OBSERVED !DATE: -----1 · □ POTENTIAL I I 01 jllf 0. CONTAMINATION OF SE_WERS. STORM DRAINS, wwrPs 02 CJ OBSERVED (DATE: -----1 )(POTENTIAL 04~NARRATIVE DESCRIPTION ! . ,ff~ ~d_fld,.__,._ ~ ./..,,,,.._.;...,4'2-,..:..__ ,,<J,,.Jl -1-o~ o---cl ot,~. O I O P. ILLEGAL/UNAUTHORIZED OUM PING o• NARRA nve DESCRIPTION 02 0 OBSERVEO(OATE: -----1 · 05 DESCRIPTION OF ANY OTHER KNOWN, POTENTIAL OR ALLEGED HAZARDS IIL TOTAL POPULATION POTENTIALLY AFFECTED: IV. COMMENTS V. SOURCES OF INFORMATION1C••-c11c,.,-,oc., .• 11.11.,•,.,.•·•.-i.•~'rM.••PO'tll /"/.. ~-;,.,.. 7 ~7 /9tf(, i ~'<) ~f ,,;is;,_,,,~ / 9 !'0 I 0 POTENTlAL . □·ALLEGED □ ALLEGED □ ALLEGED I I -------------------------~,--------------------------' ' • _.':•. '; ., : • •. . 1 S.EPA II. PERMIT INFORMATION 01 TYPEOFPERMIT&SSUED IChH• _, u..t WJOl,J 0 A. NPDES OB. UIC □C. AIR 0 0. RCRA. C E. RCRA INTERIM ST A TUS □ F. SPCC PLAN 0 G. ST A. TE,._.,, 0 I. OTHER rSHc#,J · 'rrfJ. NONE 11!. SITE DESCRIPTION , 01 STORAGEJOISPOSAL (CMell .. lN1-,,oJy/ J{ A. SURSACE IMPOUNOMENT 0 8. PILES . 0 C. DRUMS. ABOVE GROUND C D. TANK, ABOVE GROUND □ E. TANK, saow GROUND 0 F. LANDFILL 0 G. LANDS.I.RM IJ H. OPEN DUMP Jl{tOTHER .5 Pllt. A(.; G-,._.,, IV. CONTAINMENT • POTENTIAL HAZARDOUS WASTE SITE SITE INSPECTION PART 4 • PERMIT AND DESCRIPTIVE INFORMATION 02 PERMIT NUMB.ER 03DATE&SSUEO CMEXPlAATIONDATE O~COMMEtlTS I 02 AA40UNT 03 UNrr OF _MEASURE O~TREATMEN!l~_,,,._,NlfJIYI Z-{.O,ooJ Po«NO.S:. □ A. INC EN ERA TION I □ B. UNDERGROUND INJECTION □ C. CHEMICAL/PHYSICAL I 0 D. BIOLOGICAL I 0 E. WASTE OIL PROCESSING D F. SOLVENT RECOVERY ' ' 0 G. OTHER RECYCLING/RECOVERY 0 H.OTHER ! ,,_,,,, L IDENTIFICATION 01 STATE I 02 SITE NUMBER Al c__ I P o 9 c; ,1 !: f? c:-z. 7 050THER X A. BUILDINGS ON SITE 06AAEAOFSlTE $ - 01 CONTA.INMENTOF WASTESIOteU-1 0 A. AOEOUATE, SECURE D B. MODERATE I ){c. INADEQUATE. POOR 0 0. INSECURE. UNSOUND. DANGEROUS 02 o::sCRIPTION OF DRUMS, DIIONG, LINERS, BAARIERS, ETC. l ~ /4,<}"4 f:_._ ./44 Al.µ..,r-J 1, ~ ~ o'A r.J .ee-., 1~ I V. ACCESSIBILITY 01 WASTEEASICYACCESSIBLE: lli\YES ONO I 02COMMENTS , • l7, . _ _ _ _ · /{7_ (..I) a-,/~ ,,-_4.--<--< ,.<A--~ ·1 VI. SOURCES OF INFORMATION fC11•ao.c.1t.<1•'•••1•us. •·11· .,.,.,...,. ~:.,...,,,,s.,.POn•J (PA FORM 2070,13 (7•81) • ' I. IDENTIFICATION &EPA POTENTIAL HAZARDOUS WASTE SITE SITE INSPECTION REPORT 01 STAif,O2 SfTI; NUMBER PARTS• WATER, DEMOGRAPHIC, AND ENVIRONMENTAL DATA IV c.... Do q 5''/.:::J'Sz. 1 ' IL DRINKING WATER SUPPLY ! 01 TYPEOFDRINKINGSUPPLY 02STAnJS 03 DISTANCE TO SITE ,c,..ea n ur,k""9J I SURFACE WELL ENDANGERED AFFECTED MONITORED 7 COMMUNITY A.}( a)!( ,Jo B.□ c.□ A. '"Ill -NON-COMMUNITY c.□ o,G( o:□ E.□ F.□ B. 7. (a 1ml) Ill. GROUNDWATER 01 GROUSOW/t,TEAUSEtNVICINJTV~-J I 0 A.. ONLY SOURCE FOR DRINKING j(s. DRINKING I 0 C. COMMERCIAL.. INOUSTRll.l. lRRIGA.TION □ 0. NOT USED. UNl.lScAS1.E ~-.....,., I fLln'!.o.-.r•-•••-•J COMMERCIAL. NDUSTRlAL.. IRRIGATION {Noou.t __ .,_......_, I I 1.1Ji5 f s/>'i//Je) (~) 02 PCPUU.TIONSERVEOBYGROUNDWATE'A 03 DtSTANCETONEARESTORINKtNG 'NATER waL /, fr, 1ml) 04 CEPTH TO GROUNDWATER 05 DIRECTION OF GROUNDWATER Fl.OW De DEPTH TO AOUlFER 07 POTENTIAL. YlEU) 06 SOLE SOURCE AO\RFER I OF CONCERN CF AQUIFER :B::-:i::1 (ft) t.,f SE I 4tp-,,y35 (ft) ~-~ J);'YES □NO . OiOESCAIPTIONOFWEU.St~~.OHffl.lllld~IMl~topeoulsUClflrtd~IJ I . a ¥ ~ ~ . 3 'f: ~ 1s-o' (j.J,J,tv,,,,,,. . ...,~ ~ ,;5 I,, 802.'.,,;.._,_,~. '{;).. ,c,i, ,. . . _..,/4...)-,.< ~-,,(.,,~=II~~. ·-,. j ~ ~C,«-€,M4-<-. ' 10 RECH/t,RGE AREA 'I 1 1 DISCHARGE AREA }:i.vEs COMMENTS . I DYES COMMENTS □.NO _ d~~~~ /.,, ;'.•-~t~~ ~ □NO ·---·-- iV.SURFACEWATER V u • I Oi SURFACE WATER USE,c,,.~-l I )( I>.. RESERVOIR, REC!'IEATION □ 8. IRRIGATION, ECONOMICALLY □ C. COMMERClk!., ll~DUSTRIAL 0 O. NOT CURRENTLY USED . DRINKING WATER SOURCE IMPORT ANT RESOURC~S - 02 AFFECTEO.'POTENTIALL Y AFFECTED BODIES Of WATER I N,.ME: I AFFECTED 01ST ANCE TO SITE £Li &vu.h D I, 5' (ml) I □ (mo1 --□ (mo1 ' V. DEMOGRAPHIC ANO PROPERTY INFORMATION ' ·- 01 TOT.1.1. POPULATION WfTHIN t,f. /3.,,Ja,.,/.J......,_ t,,,.._.f.(!!. 3.d~p,_.f.,.~ C · 1:,, _,;e TO NEAREST POPI.U.ATION ONE ( 1) MILE OF SITE TWO 12) MILES OF SITE THREE (31 MILES OF SITE A. 15~ a. J07t_ 6. 565i. 0 (m;1 MO, OF PERSONS HO, OF PERSONS I NO OF PERSONS ... - 03 NUMBER OF BUILDINGS wtTHIN TWO (21 MILES OF SITE I 04 DISTANCE TO NEARE.t· -'. Cf-F0 Sl'r.: BUii.DiNG f O 1/= 1 'fl ,,,_ t !.{'/ . I a (mi) 05 POPULA 1 ION WITHIN VICINITY OF SITE ,,.,o.,69 ,..,,,.i, ... CMIC,_,,,_ otMI-ot--,.,,; ,..._ ..citlr ol LO, ••If••"""· .... ". : ,.. :Jy pop,,Mle(I urti.n~M) __/;& _;~ -I 9 Jo,c,--..,1". 'l/1'7'-~fa./; cJ>-,r>-C-'-4-/ .?,, 6 d<l ~(/"(I, . -"-"'-" I ' I I fl-'A FQC\IJ. 2070,13 (7•81) POTENTIALIHAZAROOUS WASTE SITE SITE INSPECTION REPORT • I. IDENTIFICATION 01 S1A.TE]02SITENUMBER ~EPA PART 5 • WATER, DEM0°GRAPHIC, AND ENVIRONMENTAL DATA . . : A/C. I A oq,.,-J/.9J5Z7 VI. ENVIRONMENTAL INFORMATION 01 PERMEABILITY OF UNSATURATED ZONE ,C,..C. OtWJ □ A.. 10-• -10-• cm/&ec 02 PERM~BII.ITY OF BEOROCK1Cllieca _, □ A. IMPERMEABLE IL•ANn rc1-6 owull'C,I □ C. 10-• -10·> cm/NC □ 0. GF\EATERTHAN 10->cm1 ... : Kc t,,f, □ B. RELATIVELY IMPERMEABLE C. R:LATIVEL Y PERMEABLE □ D. VERY PERMEABLE ,,o-4 -,o-•c:,w .. cJ t10-'-,o-• CIWUCJ '~",,_ 10•1 -.-.., I C3 C;?TH TO BEDROCK 04 DEPTH OF CONT .A.MINA TEO SOU. ZONE 05SOILpH , :2:i, -I :z. 2. t,f ~ ' 1111 I lttl ~- ' 06 NET PRs.CtPITATION 07 ONE Yl:AR24 HOURfWNFAU. i 08 SLOPE 1/-0 (in) Qg FLOOD POTENTIAL SITE IS IN i',,.,fuc,~ YEAR FLOOOPL.AJN 11 0.STANCETOWETL.ANDS/6.eH~ ESTUARINE A, lmll 13 LANO USE rN WCINITY. 01ST ANCE TO: COMMERCIAl/lNDUSTRIAL 8. ;. '5 -~-() I~) SITE SLOPE I OIRECTION OF SITE SLOPE I TERRAIN AVERAGE SI.OPE ;.s-" S~ I .2-b ,. 10 OTHER _s.,..,..p_ ,. .. -....., ' ' □ SITE ISON BARRIER ISL.ANO, COASTAL HIGH HAZARD AREA, RIVERINE FLOOOWAY I {ml) I 1 2 DISTANCE TOCRITICM. HABITAT fo/~...,.,..-•J ----'=--Cm11 ENDANGERED SPECIES: RESIDENTIAL AREAS: NATIONAL/STA TE PARKS, FORESTS, OR WILDLIFE RESERVES AGRICULTURAL LANDS PRIME AG LANO AG l.AN0 !O 8._.,..:..,_c_ __ cmn c. _____ cmn D._...::-..3:::.... __ ,rnlJ . '\ 4 DC.SCRIPT ION OF SITE IN RELATION 10 SURROUNDING TOPOGRAPHY i A~-~ 1ou, .... c1 z:L·d' ~ VII. SOURCES OF INFORMATION ,c.,--,.e,.1,,_.,, ,.,.,.,,,.,,,.,,......,;.__.,..,., ,._,,, $EPA • POTENTIAL HAZARDOUS WASTE SITE SITE INSPECTION REPORT PART 6 • SAMPLE AND FIELD INFORMATION I IL SAMPLES TAKEN S,,.MPU: TYPE 01 NUMSEROF 02SAMPL£SSENTl0 SAMPLES TAKEN , GFIOUNDWATER SURFACE WATER i V O O - I W"5TE I ' AIR I RUNOFF I ' SPti I SOIL 9 ,, : I " " VEGETATION I OTHER ' Ill FIELD MEASUREMENTS TAKEN 01 TYPE 02C<lMMENTS IV. PHOTOGRAPHS AND MAPS 01 TYPE jr[ GROUND O AERIAL l 021<CUST00Yo/ 4,c. ",,o-/J,,us rt;;lcC;./1 ~L ' ,,._oJo,pa....,■IO'IO,~ ¾YES ONO 0-' LOCATION OF MAPS p,_, c.L,._.LJ V. OTHER FIELD CATA COLLECTED,..,_ .......... ,...._, Vl. SOURCES OF INFORMATION ,c..~ ,.,.,.,.u,. ••P·· 11■1• ,...,_ ,...,.,,.. ~''"· 11:,0,ni ,, L IOENTIFICA TION 01 STATE I 02 SITE MJM8ER N c. I r. o q .c:~:5 8 t::-2, 03 ESllMATED DA.TE ~'TSAYA&>S.E oEPA II. CURRENT OWNER(S) :;:!STREU AOORE.SStl'.0.lo•.ltF01'.•rc.J ~ • POTENTIAL HAZARDOUS WASTE SITE SITE INSPECTION REPORT PART 7 • OWNER INFORMATION I PARENT COMPANY,._, 02 D+B NUMBER 08 N.&.ME 04S,CCOC£ I ,o STREET AOORE~,,..o, locu. llFD1 •• ,c.1 I. IDENTIFICATION 01 STATE 102 SITE HUMBER /\I c__ /lo C, -J-,coc2 7 09 O+ B NU tr.I BER 11 SICC00E I 2-/ E D~ ;lj.,,,,,,,_/ J!i Ci.Y 01"""'1S 03 STREET AOORESS (P.O. lo,, IIFD 1, .re.I osC1TY 01 NAME Cl STR£Er ....oDAESS(l'.O. lo&. 1tF01, ete./ os crrv 03 STREET AODRESSIP.0 lo&, 11F01 •• ,i:.1 CS CIT'I' 6STATE 07ZIPCOOE 08 STATE 06 STATE 02 D+B NUMBER 1 CM5'CCOOE 07 ZIP CODE I 02 0+8 NUMBER I I 04 SICCOOE I I. 07 ZlPCOOE I I 02 C>♦ B NUMBER 1 04S!CCOOE I I 06STAT 07 ZIP CODE 113STATE 14 ZIP CODE INc. :t76cr2- 08 NAME 09 0+8 NUMBER 10 STREET AOCRE.SS(l'.O . .,_._ 1tf'01. MJ 11 SICCODE 12 CITY r3STATE UZIPCOOE OBNAME o; O+BN\JMBER 10 STREET AOORESStP.0. lolU. ,ir:r,,,.,c.1 11SICCOOE 12 CITY l'3STATE 14ZIPCOOE 08 NAME O90+Bt◄UMBER tlSICCODE 12 CITY r~STATE 14ZIPCOOE Ill PREVIOUS OWNER(S) ,.,.,_,_..,.. IV. REAL TY OWNER(S) ,..__,.,_,,....,_, 01 NAME 03 STREET ADDRESS ,,..0, ao.. RFD, • .cc.I 05 CITY OlS'mEET AODRESS,,..o.1o&.1tFD1.,rcJ OS CITY 01 NAME C3 STREET ADDRESS ,,..o. ao,. 11,q,. •te.l 05CITY 02 0+ B NU~BER : I 04S!CCODE I oeSTATE DTZIPCOOE 02: D+B NUMBER I 04 SICCOOE ! 08SlATE OT ZIPCOOE 02 D+B NUMBER / 04 SIC CODE I I DeSTATE 07ZIPCOOE I 01NAME 03 STREET AOOAESSf,..0.lol. IIF01,•IC.J 05 CITY 01NAME 05 CITY 01 NAME 03 STREET AODP.ESStP.O. lo•. IIFDI. ,,c.J 00C1TY V. SOURCES OF INFORMATION re., .-c.11..:: ,.,,,-... '·"·· 1111, ,..1. ~ ~-,.po,111 F? ft' 7,,,, 14 c"J ~ _;/,_J.-;;,,., to.,(<:) ls-/z./ g,;;; I ' 02: D+B NUMBER .106 STATE 07 ZlPCODE 02 D+B NUMBER O•SICCOOE I oo ST A TE 01 ZIP CODE 02 D+B NUMBER 104SK:COOE 1°6STATE 07 ZIPCOOE • POTENTIAL HIDRDOUS WASTE SITE I. IDENTIFICATION &EPA SITE INSPECTION REPORT 01 STATE102SITENUMBER PART 8 • OPERATOR INFORMATION A' c Do 9 _.,. u <<? <z..., ' IL CURRENT OPERATOR , __ ,.,. __ •-• I OPERATOR'S PARENT COMPANY ,,_, 01 NAME 02 0+8 NUMBER 1 10HAl.1E 11 D+B NUMBER FC X :./1.ftLJ-,~ n;,,1 ch,1-~ I 03 STREET ACORESS ,,..0. Sol, ltFD I, ~c.J 0' SIC CODE I 12 STREET ADDRESS ,,..0, ~-IIFD ,. •re.I 13 SlCCOCE /02-0 /,(_}..,,_,,/-/';,,=, (-4./. I I 00 CITY 06 STATE 07 ZIP CODE 1' CITY 15 STATE 18ZIPCODE _j~ ;(JC.. .2.2~771 08 YEARS OF OPERATiON 0~ NAME OF OWNER ' ak,,/ ;.1t I t:=c;(. "~ ,;.._, n,,t/.__ • ...;., • ~ I ~ . ' nt. PREVIOUS OPERATOR($) ruu-rtec..w11nr;,-,,,,,..,.,,,,-,.,.,..,__,,_ PREVIOUS OPERATORS' PARENT COMPANIES ,._, 01 HAMS. 02 D1-8 NUMBER I 10N ... ME 11 D+BNUMBER 03 STREET ADORESS ,,..O.~ IIFOl.~I 0. SIC CODE 12 STREET ADDRESS (P.O.~. ltFDl.•IC.J 13 SIC CODE 05-C"TV 06 STATE 07 ZlPCOOE 14 CITY 15STATE 1&ZIPCODE oa '!'EARS OF OPf;u. TION 08 NAME OF OWNER CURING THIS PERIOD 01 N"ME 02 D+B HUMBER 10N ... ME 11 0+ 8 NUMBER ' 03 STREET AOORESS(P.O. llol:. ~DI, etc.I 04SICCODE 12 STREET ADDRESS ,,.,0, eo&. AFD •, •rcJ 13 SIC CODE ····---~-----·-·······-~ C! CITY j 06 STATE 07 ZJPCODE 14CITY 1!1STA.T2 16ZIPCOOE 06.YEARS OF OPER-.TION 00 NAME OF OWNER DURING THIS PERK>O Cl Niu.~ 02 D+B NUMBER 10NAME \ \ 0♦8 NUMBER 03 STREET A!:IORESS ,,..0. aoa. a,-o •. n:..J 04 SiCCODE 12STREET AtlOAESS fl'.0.1o&.RF01.--, 13 SIC CODE I o~ err, OD STATE 07 ZIPCOOE I 14 CITY 15STATE 19ZIPCODE I OB YE.\RS OF OPEP.A.TION 00 NAME OF OWNER DURING THIS PERIOD i I'/. SOURCES OF INFORMATION 10t,11Md1e,.,,,_..a.,.11 .. swi.,..1,.--~ ... """J ~ p--J1J: I I I ' I I ' I I I ' ~EPA POTENTIAL HAZARDOUS WASTE SITE I. IDENTIFICATION SITE INSPECTION REPORT 01 STATE102SfTEHUMBE.R • PART 9 • GENERATqRJTRANSPORTER INFORMATION Ne D 0°.c;:<1,;Ju-2-, IL ON-SITE GENERATOR ' I .. 01 NAME 02 C>+B NUMBER I ! 03 STREET ADDRESS ,,-.0. lo&. NO•. erc;.J CMSICCOC>E ' ' . OSCITY oe STATE 07 ZIP CODE I I ' Ill. OFF-SITE GENERATOR($) ' I 01 NAME 020+BNUMBER I 01 NAME 02 0+8 NUMBER I 03 STREET ADORESS tP.0. ao.., llf.FOI, etcJ CMSICCOOE 03 STREET ADDRESS IP.O.lol:.ltFOI.~ °' saccooe. OS CITY 06 STATE 07 ZIP CODE OS CITY O&STATE 07 ZIPCODE C1 NA.ME 02 D+ 8 NUMBER 01 NAME 02 D+B NUM6ER 03 STREET AO DRESS tP.O. ~ RFD,, .ic.J 04 SlCCODE 03 STREET A00ReSS (P.O. aoa, NOi, NC.J 04 SICCODE 05CITY 06 STATE OT ZIP CODE OS CITY 06 STATE 07 ZIP CODE IV. TRANSPORTER(S) ' 01 NAM£ 02 0+8 NUMBER ' 01 NAME 02 0-.-8 NUMBE.R I ' 03 STREET ADDRESS tP.0. tu AFO ,. -.1 04 siccooe I 03 STREET ADORESS fP.O.~IIFDI.-..J 04 SICCODE I I OS CITY 08STATE 07 ZIPCOOE I OS CITY e>eSTATE 07 ZJPCODE ! 01 NAME 02 D+B NUMBER ' 01 NAME 02 D+BNUMBEI\ I I "03 STREET ADDRESS fP.0. lo&. ltFOI, iMc.J 04 SICCOOE ' 03 STREET ADDRESS fl'.O.aci1.1IF01.'1fe..J 04 SIC CODE : 05 CITY 06STATE 07 ZlPCODE I 05 CITY 06$T4TE 07 Z!PCODE .• I V. SOURCES OF INFORMATION ,c .. u~c,...-.r.e.,.,.,..-.,.NffOll~,n.,.:,oi,•J I I . ' I I I ---/ I ! . 6EPA POTENTIAL HAZARDOUS WASTE SITE SITE INSPECTION REPORT PART 10 • PAST RESPONSE ACTIVITIES IL PAST RESPONSE ACTIVmES 01 0 A. WATER SUPPLY CLOSEO 0< DESCRIPTION 01 0 8. TEMPORARY WATER SUPPLY PROVIDEO 04 DESCRIPTION 01 0 C. PERMANENT WATER SUPPLY PROVIOEO 0< DESCRIPTION 01 0 0. SPILLEO MATERIAL REMOVED 04 CESCRIPTION 01 0 E. CONTAMINATED SOIi. REMOVED 0' DESCRIPTION 01 0 F. WASTE REPACKAGED ~ DESCRIPTION 01 0 G. WASTE DISPOSED ELSEWHERE o, DESCRIPTION 01 0 H. ON SITE BURIAL 04 DESCRIPTION 01 0 I. IN SITU CHEMICAL TREATMENT O< DESCRIPTION 01 0 J. IN SITU BIOLOGICAL TREATMENT 0' DESCRIPTION 01 0 K. IN SITU PHYSICAL TREATMENT o, DESCRIPTION 01 C L ENCAPSULATION 0' DESCRIPTION 01 0 M. EMERGENCY WA>ffE TREATMENT o, DESCRIPTION Cl O N. CUTOFF WALLS • 04 DESCRIPTION 01 0 0. EMERGENCY OIKING!SURFACE WATER OIVERS!ON ~ DESCRIPTION Cl O P. CUTOFF TRENCHES/SUMP o, DESCRIPTlON 01 W 0. SUBSURFACE CUTOFF WAU. C·C DC~RIPTlOhl ' 1020ATE I02DATE I020ATE 102DATE !02 DATE _____ _ I 102 DATE I '02 DATE I I '02DATE 02 DATE ______ _ ;02 CATE ______ _ ,02DATE ;02 DATE ______ _ ! 02 DATE I 02 DATE ______ _ 02 DATE 1 02 DATE 02 DATE I L IDENTIFICA TlOH 01 STATEl 02 SITE NIJMBcR N c. ID O Q,-..,t,z,;-z 7 03AGENCY 03AGENCY _________ _ 03AGENCY _________ _ 03AGENCY 03AGENCY __________ _ 03AGENCY 03AGENCY 03AGENCY 03AGENCY __________ _ 03AGENCY __________ _ 03AGENCY 03AGENCY _________ _ 03AGENCY 03AGENCY _______ __;_ __ _ 03AGENCY _________ _ 03AGENCY 03AGENCY • &EPA POTENTIAL HAZARDOUS WASTE SITE L IDEHTIFICA TION SITE INSPECTION REPORT 01 STA.le.I CZ S.'TE NUMS1:R PART 10 • PAST:RESPONSE ACTIVITIES Ne ooq5.;c-35z7 n PAST RESPONSE ACTIVITIES.,_ ! 01 D R. BARRIER WAU.S CONS11'1UCTED :02DATE 03AGENCY O• DESCRIFTlON I 01 D S. CAPPINM:OVERIN<l '02 DATE 03AGENCY o, DESCR!PTION I 01 D T. BULK TANKAGE REPAIRED 020ATE 03AGENCY 04 DESCRIPTION I I 01 D U. GROUT CURTAIN CONSTRUCTED 02DATE 03AGENCY 04 DESCRIPTION I 01 0 V. BOTTOM SEALED :02DATE 03AGENCY 04 DESCRIPTION I 0~ 0 W. GAS CONTROL 02 OATE 03AG5NCY 04 DESCRIPTION ,· I . 01 w X. FIRE CONTROL 02DATE 03AGENCY 04 DESCRIPTION ' I I 01 D Y. LEACHATE TREATMENT !)2 DATE 03AGENCY 04 DESCRIFTlON -·--------· --,. ... I I 01 D Z. AREA EVACUATED 02 DATE 03AGENCY - 04 DESCRIPTION ' ' 01 D 1.,ACCESSTOSITERESTRICTED · 02DATE 03AGENCY 04 DESCRIPTION I . I I 01 D 2. POPULATION RELOCATED 02DATE 03AGENCY 04 DESCRIPTION I ' . ' 01 0 3. OTHER REMEDIAL ACTJVITIES 02 DATE 03AGENCY 04 DESCRIPTION . . I r. c. fl,.,, f .-vvvVf4l'f!~ (.,<-10,d..t; ~ ,c1,--d ,,;,._,,,t.,d.c,l r ~ ,t,,,...,,·d c.udlc "· I I I . . I I I ' Ill. SOURCES OF INFORMATION tCii• l~C ,.1.-.c. • Cl .. Slat•,-,,.......,,. -rM. l•POtll/ I F C. ~r 4"71 ,,t..? r~ 19,tb -~ dhdd .,,__,.,._, ~,._rf. I ' I I I ' S.EPA II. ENFORCEMENT INFORMATION POTENTIAL HAZARDOUS WASTE SITE SITE INSPECTION REPORT PART 11 • EN~ORCEMENT INFORMATION ' 01 ;,AST REGUU.TORY/ENFORCEM...~ ACTION □ YES ){NO CZ DESCRIPTION OF FECERAI... STATE. LOCAL REGULATORY/ENFORCEMENT ACTION 7u,,,u_ ~. ' I Ill. SOURCES OF INFORMA. TION ,, .. IP«#C ,.,.._ .. , •·'1·· .,., ....... ~ ..... ,, .... '9POlt1J L IDENTIFICATION DIVIS ION QF ENVIRONMENTAL MANAGEMENT G_ROUNDWATER SECTION April 7, 1986 MEMORANDUM TO: Bill Meyer Head, Solid & Hazardous Waste Management Branch FROM: Perry Nelson ~ / Chief GWS jfl/ SUBJECT: Alleged Burial of Pesiicides; Incident #3172, FCX Statesville '· Plant, Iredell County 1 ' Please find attached for your information a memorandum from Jessie Wells / of our Mooresville Regional Office. An official of FCX has reported to Mr. Wells that 5,000 to 10,000 pounds of pesticides are buried under a portion of a warehouse. The regional o(fice is being advised-to have the company's. consultants, Rose and Purcell of1 Fayetteville, prepare and submit a plan for the determination of the extent 6f groundwater contamination and subsequent remediation. · I Should you have any questions concerning this incident, please contact Bill Jeter or Douglass Dixon in this office (733-5083), at your earliest convenience. PFN/bjg cc: Incident Files • I 3 March 19 86 I TJ: Lee Crosby F?.ON: Grover Nicholson RE: Additional CERCLA Site ' Please request that EPA add the following site to the ~:1...~IS list. ' Site Name: ?CX -S~atesville ' Address: 1620 West 1 Front Street City: Sta':.esvi lle, , NC 28677 County: Iredell State: North Carolina County Code: ~9 , Congressional Distr~ct: 09 Site Discovery Date/ 26 February 1986 I Contact Person: Gro,ver Nicholson/Earry Holladay I Narrative: This facility, closed and in ':.he process of' being sold, began operations in about 1940 as a d~stribution center for pesticides. Later, pesticides were formulated and\ mixed on-site. A former PCX manager repotted that an on-site burial of S, ,DOD -10,000 pounds of DDT, T;:>E, and chloidane occurred in 1966. The pesticides were buried about 10 feet deep and later, a concrete floored warehouse whs built over the burial trench. During an investigation of the site by a private company, four groundwater monitoring . ' wells were installed and the water sample from at least one was found contaminated with Lindane. Although the area is used by light industry and is served by the Statesville water supply (surface source), the Carnation milk plant adjacent to the FCX property us~s a well for truck wash-do~n water and other purposes not connected with their production process. rt· is possible tha~ ot~er con~amination may exist ontsite because feedstock che~icals and e:::otv ::r,emical drums were stored and handled there. .. -! Groundwater and soil contam~nation by pesticides is suspected. There have been no cleanup or enforcedent actions. I'he site is ?resently .being investigated for contamination dy the NC De?artment of Agriculture and NC Division of Environmental M~nageme~t. I Gtl/tb/0176b ' 28 February 1986 I TO: File FROM: Harry P. nolladay RE: PCX -Statesville I called for Mr. narold Fulp, Director of Statesville Water System [(704) 873-7671]. ~r. Steven Lamberf answered questions in Mc. Fulp's absence. The water system serves about 30,000 people (population of Statesville is approximately 19,000)~ Their water intake is on the South Yadkin River about seven miles NNW of the center of Statesville. I HH/tb/0176b Tu: FROM: RE: File Harry P. Holladay FCA -Statesville • I 28 February 1986 ' I contacted 11r. ·william H. :McCullough regarding the subject site. Hr. i1cCullough is handling the legal I aspects. ·rhe identif icaticn is FCX Inc., Debt in Possession in U.S. Bankruptcy Court for Eastern District of NC s-85-Ul574-5. southern States CooperativJ Inc, of Richmond,. VA authorized the Hart study. 11cCullough learned 2/17/86 that southern States we,uld reject purchase of site because of heresay of contam{nation levels on site. McCullough said ' that a second opinion should be rece±yed, Fisher and Percell were contacted ' . to be consultants. Bankruptcy court ·approved of the two consultants. The Hart report is over due but not in. ~ark Morrell (with Hartl indicated that it was to be sent by express 2/24/86,'1 It is now hoped to be here 3/1/86. Regarding sampling: good. Groundwater data may be HH/tb/0176b ' surfac~ contamination I suspec~. ! information probably •• .. I. IDENTIFICATION 6EPA POTENTIAL t~AZARDOUS WASTE SITE PRELIMiNARY ASSESSMENT 01 STATE!02SlTENUMBEf4 NC I t)C1S,;i:,8S27 II. SITE NAME AND LOCATION 01 SITE NAME,~~. com,not1. o, oerc:noti.-. ,,_ of M•J 03 CITY Statesville 09 OOOROlNATEt. ·-LAmUOE ..35. 4:1_ QL._ I 10 D:fiECTJONS TO SITEISl•:i,ng tromi,NrHIDllt>JfC -01 PART 1 • SITE IN~ORMATION AND ASSESSMENT· 02 STREET, ROUTE NO., OR SPECIFIC LOCATION IDENTIFIER 1620 West Front Street 04 STATE 105 ZIP CODE 1'06 COUNTY NC 28677 Iredell 1 07COUN 1"1'08 CONG CODE DIST 49 9 LONGITUDE l JJBD_ 55...... lD_.L Take I-40 to (on NC'/0). I Statesville, turn.south on NC. qo and continue to 1620 West Front Street I 11!. RESPONSIBLE PARTIES 01 OWNEFi/UkfJ0-.,1• ~-~~-·1~"c·.•i;:~k~:tt···· .. CITY . _ tatesville" ·-· '·· 02 STREET (&,u,u..s. ,.,...,a, ntllO'•~/la.? 1620 West Front Street 04 STATE{ 05 ZIP CODE 06 TELEPHONE NUMBER NC I 28677 17041872-5261 I O 7 0Pi;AA TOR /1:' ~,.,, ... ~ ~ tNl•r•11t from ow111r} ·~•-·~~-•1,'-'.1',:t,~..;• • ·•~-. , ..... ·;::~f~rt1B~t;~tr> 1'.!l:·ti;..f;':~~'> ... •' -:✓:~ • 09CrrY 10STA.TEl11ZJP~OE 12 TELEPHO~E NUMSER I ) iJ1¥PEOFOWNt:: HIP(O-a011eJ I A.PRIVATE·□ e:FEOERAL: _____ ._._, __ l~----- lAp,,ncr_, 0 C. STATE DO.COUNTY 0 E. MUNICIPAL 0 F OTHER . . . .. . . ···-·--· . ! . -··· . 0 G. UNKN.OWN -~.-.., ...... r.c,.:-:~,::;;;:;;;;cc.;;i~;':,o=:ef..Ei;;RA,:'oro". R;;;"Na:·-;,,,TI"f"r~,'-~;;-;,;ON;,,---;,::--~;;,.;;---L£,.-~..,-,"""';;::.,,.,~.,,-.. ::,:::,_,,::c,_,-"-,l"''-,::::::::::::::::;::::::::::::::::::::;:-_______________________ -l C A: ACRA 3001 "DATE RECEIVED:""· · · .-' ' D e.'uNc0NTROLLEOWASTE SITErcERCLA 10,~1 DATE RECEIVED: , , MONTH DAY VEAR MONTH OAY YEAR f(c.NONE IV. CHARACTERIZATION OF POTENTIAL HAZARD 01 ON SITE U-!SPECTION av~ .. ,,,.,~,: 0 YES,,_ DATE-,=,,·,,_·' =c'·''=,.,·-· •. 0 A. EPA · .• ·· ,,.□ B.EPACONTRACTOR 0 C.ST~TE •.. 0 D. OTHER CONTRACTOR . :. . • •. ~ NQ,.-•-: '. MONTH .DAY., YEAR ·····--0 E. LOCAL HEALTH OFFICIAL . 0 F. OTHER: • "" 1 •:i ·,, , ,,. ·1 . ••'• . ··••· -'· -------,~---,,-------.. "• CONTRACTOR NAME{S): G2SITESTATUStc-ca:-i . . 03 YEARS OF OPERATION . . o A. ACTIVE '\l(e. INACTIVE · □ c. UN-KNOWN--"~ ?:::.,, ::-~r · ·"' 1240 = -1 19 69 ·-. ·---··-0 UNKNOWN··•-- •• • . ~INGYEAA ENDING YEAA 04 DESCRIPTION OF SUBSTANCES POSSIBLY PRESENT, KNOWN, OR ALLEGED EPA Establishmerit·. to manufacture or re'pack pesticides -repacking included DDT, TDE; Lindane, Chlord~1:e·, Mala th ion, Aldrin.I Heptachlor, and tobacco. spray_ (pro~ably MA-30 types). Liquids repackaged 1965-1966, dusts up to 1969. Seed treating with Hg ,... .JC' -____ .... _.J, . • 05 DESCRIPTION OF POTENTIAL H"2A.RD TO ENVIRONMENT ANO/OR POPULATION Mr. Reed, FCX manager, indicates that 17-10,000 pounds of DDT and TDE are buried in a hole"-~ten· feet -deep .. under. the present warehouse. Area for empty drums potential hazard Waste taken· to city.landfill in plastic bags. Site on city water, but four monitoring ' .,,,... ... ,.. •-a ---~..;,.....;..:1...,._.. ..;..:1--"'·.l..:4=..;-..1 --~ c::c:: __ 1.. Lindane. Well at adiacent V.PRIDRITYASSESSMENT r--C.-•0 on nlant not 'contaminated and not used in food processing. 01 PRJQAITY' FOR INSPEC. TION(Chec:1rone-:;,g/lor~11e1>ected, c:°"""91• Pan 2 • ~ni, ln/orrn,!ICW'landPett. 3 •O..et¥1t.onolHeur001.11 Col'>dl!OOt'11-mc1CHri111 0 A. HIGH · • • · · · ·• ~ B. MEDIUM · 0 C. LOW O D. NONE . , /ln-uo,r --.aproniotly) .::. · (,\olt,0.c:l#Olt ~HI· f/Jn~cl c,,, ,,.,,.. ,...,.blol b41sll/ , /Na flltff',,et eel""' 1teeded. con1p1t,1e c.,,,.-,11 dl$pOII!...., lomt) VJ. lliFORMA TION AVAILABLE FROM 01 CONTACT OJ TELEPHONE NUMBER Lonnie Reed, Manager 1704 )872-5261 os Pf:.RSO~ FiEs:-o:-..s1aLE !="QR ASSES..<:;MENT OS AGENCY 06 ORGANIZATION 07 TELEPHONE NUMBER OB DATE H. Holladay/G. Nicholson NC DHR!/DHS SHW Mgmt. Br. &191733-2178 02 ?8 186 1,,10NTH 0AV YEAR I All water reports considered preliminary at this time. •• -l POTENTIAL HAZARDOUS WASTE SITE I. IDENTIFICATION &EPA PRELIMINARY ASSESSMENT 01 STATE ,~2 SfTE NUMBER PART 2 • WASTE INFORMATION Nr I ll. WASTE ST ATES, OUANTITIES, AND CHARACTERISTICS ' .:n PrffSIC/>.J.. ST ATES ,c~.cqJ</M/.,,0,,J 02 WASTE QUANTITY AT SITE 03 WASTE CHARACTERISTICS 1C1>1>Ck., rna1 aw,, 1,., .. ,.,,., ol •ast• ouati,,._ X •. TOXIC ){ E. SOLUBLE I ;: :,... 50Li0 :.] E. SLl.'FIRY "'J$I IH "'~-0 0 I. H1GHL.YVOLATILE :.-. !l P:JV,r:::>EJl, FlNES XF.'..IC'.:!:::i TONS ..,. 5 0 8. CORROS!I/E 0 F. INFECTIOUS 0 J. EXPLOSIVE L C. SLUDGE ~; G. GAS 0 C. RADIOACTIVE C G. FLAMMM!:..E U K. REACTIVE ... -CUBIC VAROS !J 0. PERSISTENT OH.IGNJTABLE 0 L. INCOMPATIBLE • . .: :J OTHER tJ M. NOT APPLICABLE .. fS;:~-;,'): ::O.OFO!'l'JMS tll. V/A$'i(; TYPE CA":=G-'.)A'r SUBST AN.::::E NAME 01 GROS!; AMOUNT 02 UNIT OF MEASURE OJ COMMENTS SLU SLUDGE OLW Ol~YWASTE SC'L I SOLVENTS r-(n) PESTICIDES 7 10 ,00( pounds Pesticides in soil and ground . :,., - C:CC OTHER ORGANIC CHEMICALS . .. water 1 fioc J INORGANIC CHEY.IC.A.LS DDT, TDE, Lindane, Chlordane, ~co ' ACIDS Malathion, Aldrin, Heptachlor, I I 3;...5 : BASES and tobacco sprays (probably 1-.lES HEAVY METALS MA-30 types) . 1'/. l-:A'ZARDOUS SUBSTANCES /SoA:~N11~/01°mo.ltr.ou.,,i,yc,iaiCASN<.trrttw,sJ Hg possible from seed treatment. C1 C_.,TE.GOAY 02 SUBSTANCE N•ME 03 CASNUMBER 04 STORAGE/DISPOSAL. METHOD 05 CONCENTRATION 06 MEASURE OF CONCENTRATION .-. " .. . -.. ' .. -. ..... . ,.~ .. . .. . -, -. -. . -. .. L . -· . •. I .. ..... . -. .. -. . -~--. · . ... . V. F.!:.!:OSTOCl(S ,s,.• ,-,o,na., 10,C.-S N.....,u,,s) ,C.i..iEGC·M1 01 f.EE:OSTOCKNAME 02 CA5 NUMBER CATEGORY 01 FEEDSTOCK NAME 02 CAS NUMBER f'DS FDS FDS FDS FCS FDS FD3 FDS I VI. S\JURC~S OF INFORMATION ,c,r,spf'cll,cralatancas.•-a. 1111:a ,-.J, J91"!0III 11r.a1y11s. fflPOrTS ) l. John E. Hunter III, Assistant Head of FDA Department of Agriculture, Pesticides Branch, 3-3556. 2. Jesse Wells, DEM Mooresville Groundwater. (7()_4) 663-1699. I t.... .............. ,. ··-· ...... ~. -~ •· . . .. POTENTIAL HAZARDOUS WASTE SITE I. IOENTIFICA TION @EPA PRELIMINARY ASSESSMENT 01 STATE I 02 SITE NUMBER . "~ n PART 3 • DESCRIPTION OF HAZARDOUS CONDITIONS AND INCIDENTS 11. HAZARDOUS CONDITIONS AND INCIDENTS I 0 l ,C. A. GROUNOWA TER CONTAMINATION 02 !J OBSERVED {CATE: I 0 POTENTIAL ){ALLEGED 03 POPULATION POTENTIALl ':' AFFECTED: Unknown 04 NARRATIVE DESCRIPTION Trace pesticide contamination in monitoring wells indicated in initial tests- more tests under way. Well at adjdcent site not contaminated at this time. i 01 1 t~· SURFACE WATER CONTAMINATION 02 0 OBSERVED {~ATE: I }l:l POTEtmAL 0 ALLEGED 03 PULATION POTENTIALLY AFFECTED: 04 NARRATIVE DESCRIPTION I No known population potentially af~ected. ! O~~ C. CONTAMINATION OF AIR 02 C OBSERVED{OATE: I ~POTEtmAL 0 ALLEGED 03 PULATIONPOTENTIALLYAFFECTEO: Unknown 04 NARRA nve DESCRIPTION I Air contamination inside the buildings on site I may occur. I 01 0 0. FIRE/EXPLOSIVE CONDmONS 02 .□ OBSERVED {CATE: I 0 POTEtmAL 0 All.EGEO 03 POPULATION POTENTIALLY AFFECTED: 04 NARAA TlVE DESCRIPTION ' I I 01. ~ 1 E. DIRECT CONT ACT Unknown 02 0 OBSERVED {DATE: I ~ POTENTIAL D ALLEGED . 03 PULA TION POTENTIALLY AF~CTED: 04 NARRATIVE DESCRIPTION I Workers in the area may come in contact with the contaminated soil. I ! 01 ir CONTAMINATION OF SOIL 02 0 OBSERVEDIOATE: I 4 nr I D POTEtmAL ~ ALLEGED 03 EA POTENTIALLY AFFECTEO: ~2 04 .NARAA TIVE DESCRIPTION fAc:,.l) -· ... . ' Company manager reports burial inl hole now under warehouse. I 01 1 ~~-DRINKING WATER CONTAMINATION 02 0 OBSERVED {CATE: I )I POTENTIAL 0 ALLEGEO 03 PULATION POTENTIALLY AFFECTED: llnknQHU 04 :NARRATIVE DESCRIPTION Area on city drinking water -well;water present in area for other intended purposes. I I 01i~t··WORKEA EXPOSURE/INJURY 02'0 OBSERVED {DATE: I 1'-POTENTIAL D ALLEGED 03 ORKERS )'OTENTIALL Y AFFECTED: · Unknown . 04 NARRATIVE DESCRIPTION .. I ' Potential if site is used for business. I 01 1 ,rol, POPULATION EXPOSURE/INJURY 02 _D OBSEAVED(DATE: I )l: POTENTIAL D ALLEGEO G3 OPULATION POTENTIALLY AFFECTED: llnknQIDl 04 NARRATIVE DESCRIPTION I . ' I EP,t,. FORM 2070·12 (7-81) G (\~EPA POTENTIAL HAZARDOUS WASTE SITE L IDENTIFICATION PRELIMINARY ASSESSMENT 01 STATEI02 SITE NUMBER PART 3 • DESCRIPTION OF HAZARDOUS CONDITIONS AND INCIDENTS NC no 7:f' II S2 :,Z. 7 .!. HAZARDOUS CONDITIONS AND INCIDENTS ,co,,,--, 01 0 J. OAMAGE TO FLORA 02 0 OBSERVED (DA TE: 04 NARRATIVE DESCRIPTION ) 0 POTENTIAL 0 ALLEGED Not likely. . 01 0 K. DAMAGE TO FAUNA 04 N~TIVE DESCRIPTION ,~,._1,1o1~,1 02 0 OBSERVED (DA TE: ) 0 POTENTIAL 0 ALLEGED Not likely. 01 0 l. CONTAMINATION OF FOOD CHAIN . 02 0 OBSERVED (DA TE: ) D POTENTIAL D ALLEGED 04 NARBATIVE DESCRIPTION Not likely. . --•· -.. .. . . . . 01 0 M. UNSTABLE CONTAINMENT OF WASTES . . 02 0 OBSERVED (DA TE: ) 0 POTENTIAL 0 ALLEGED (S(Ji#s,',unolf.'sl....a,,,g jqu,dsl~p dn.msJ 03 POPULATION POTENTIALLY AFFECTED: Ilnkna:w:n 04 NARRA T1VE DESCRIPTION -. . .. : .. : . -. .. -... .: . : . 01! N. DAMAGE TO OFFSlTE PROPERTY ... 02 0 OBSERVED (DATE: I . X POTENTIAL 0 ALLEGED 04 ARRA TNE DESCRIPTION . Contamination migration to adjacent food processing plant or others nearby could result.· ,----··· ·• -··--------·-.... . .. _ --... . .. ,. - 01 ~-CONTAMINATION OF SEWERS, STORM DRAINS, WWTPs 02 0 OBSERVED (DA TE: · ) )il.POTENTIAL 0 ALLEGED 04 RA TIVE DESCRIPTION . , .. Drains are on site •. ·•-._.,,. ___________ ---··-···--···-. ----------------. -~--... -. -........... , .. I it:...'. ..•. .. .. ,,-,. ... , ...:: :., . . ' . ... -.... •.· . 01 0 P. ILLEGALJUNAUTHORIZED DUMPING 02 0 OBSERVED (DATE: ) D POTENTIAL 0 ALLEGED 04 NARRATIVE DESCRIPTION -. -•· .. -----· .. . .. .. . .. . . .. . . . . .. --. - 05 DESCRIPTION OF ANY OTHER KNOWN. POTENTIAL. OR AU..EGED HAZARDS ... ... . None known. .. IIL TOTAL POPULATION POTENTIALLY AFFECTED: IV. COMMENTS .. , . . ... .. . ! V. SOURCES OF INFORMATION (Cl!UC-Cif/Clfl••MCH,■.g SI-0.. . ....,.. ....,., ... , ,-!SJ ' I As previously cited. ' j -l (;•A fC-fiM 2070•12 \7•61 J • • 27 February 1986 I TO: rile FROM: Harry P, Holladay RE: FCX -Statesville I called C. Page Fisher, NC 27707], consultant for Rose and received the following information: ['( 919) 493-1815, Box 8761, Durham, I Percell Inc. [(919) 323-3400], and I I I FCX is in bankruptcy, Mr. William H. McCullough of Sanford, I Adams, McCullough, Beard, is the legal council. I . . I Only tele;,hone and verbal information is available in some areas until report from Hart Assoc. (P •. Watts) issued. I I Available information in,dicates 8ppb Chlordane and 26ppb DDT. in soil. 'rhis may be a composite sample. I I Sampling techniques may be a problem with well samples. Water contamination may have resulted from drilling through contaminated soil, from Using a contaminated auger, and from ' leaks in bad joints in PVC well casing. Unconfirmed reports of 58ppb Lindane in the gro~ndwater are circulating. I I Seed cleaning was also c~nducted at this site, (Seed cleaning often utilizes mercury compounds for preservation). I Rose and Percell will geJ a copy of the first program requested by Southern States via Fr1ed c. Hart. I I Jesse Wells to get groundwater log for the Carnation Plant well. Only storage gasoline and I tanks known to be on the site are 7500 gallon ' 10,000 gallon diesel fuel tanks. I NCDA insecticide inspector sampled at the Carnation Plant. I I Lonnie Reed is now employed by Southern States. He was a manager for FCX. : The FCX site is a long nar•row strip of land bel;.ween Front Street and the railroad. The I is estimated to be about five are,a acres. Building size is about 2201' X 4 60' • I • • -Rat bait was repackaged on site in the 1980's, I -Site called FCX uistrioution Center. Site repackaged and distributed to other FCX units. I Carnation Plant is upgJadient from the FCX plant. suggested contacts: B. aruce Williams/John~-McGlamery I Division. [(919) 733-7366] FDA -Food Mr. Lonnie Reed, past m~nager of FCX, (704) 872-5261 or 5262, ! Jesse Wells with DEM. HH/tb/0176b TO: FROM: RE: • File Harry P. Holladay FCX -Statesville NC D095458527 • 27 February 1986 I spoke with John E. Hunter III, North Carolina Department of Agriculture Pesticides Branch (733-3556), regarding the subject site. The following information was received: FCX site was a registered EPA Establishment for manufacture or repackaging of pesticides. FCX started operations about 1940. Mr. Lonnie Reed was FCX manager for site. Mr. Reed indicated that 7,000 -10,000 pounds of DDT, TDE, and Chlordane were placed in an on-site hole approximately 10 feet deep in 1966. The pesticides were covered with soil and subsequently a warehouse with a concrete floor was built over the area. During 1965-1966 pesticides were repackaged at the site. These included DDT, TDE, Lindane, Chlordane, Malathion, Aldrin, Heptachlor, and tobacco sprays (MA-30 types probably). No pesticides were buried on site since Mr. Reed became manager in approximately 1966. Four monitoring wells were drilled 40 -60' deep by a contractor, Fred c. Hart Assoc. Inc., of Washington, DC. Three wells are downgradient and one is upgradient. c. Philip Watts is the hydrologist. The wells were sampled 10 February 1986. All wells have PVC pipe casing and were drilled with the same auger. Repackaging operation consisted of breaking contents of 55 gallon drums and 50 pound bags down into smaller containers of product for sale. Packages taken to landfill when empty. Powdered product was 50% active. 'Empty drums were stored on the site until a reconditioner picked them up. One of the wells is located at the old drum storage area. HH/tb/0176b North of the site acros~ the railroad 1s a Burlington Plant. The ' Carnation Plant, and sereral other business buildings are just to the west of the site. ~he immediate area is primarily used for industrial purposes, particularly by electronics and paper ' industries. The site slopes 945' above HSL. I gently from East to West dropping from 965' to The Carnation Plant is upgradient of the site. I The soil i.s sandy. The;monitoring wells reportedly produce about 500 gal/min. ' PVC pipe was used as well casing and duct tape was used to join the sections of casing in the monitoring wells. ! The water levels are 35\ to 40' below land surface in the wells. • 27 February 1966 Tu: File FROM: Harry P. Holladay RE: FCX -Statesville I called Mr. Jesse Wells, DEM ( 704) 663-1699, and received the following information about the subj~ct site: HH/tb/0176b I Liquid repackaging was ~topped in 1966. Dust repackaging was stqpped in 1969. Philip Watts report (wj.~h Fred C. Hart Assoc.) is due this week. Mr. Wells is sending le~ter of request for water quality data. I . Dust wastes were sent t~ the old Statesville landfill (city or county not known). There are probably only two storage tanks on the property -for gasoline and diesel fuel~. The other information tehded to confirm that in the John E. Hunter communication. I • I 27 February 1986 TO: File Harry P. Holladay RE: FCX -Statesville Mr. E. Bruce Williams, 733~7366, FDA Food Division, returned my call. He indicated that groundwater I samples had been analyzed but that he had not seen the results. Mr. Williams ~ill phone as soon as he receives results. He also indicated that the \adjacent Carnation plant uses city water in their process but well water for truck wash down and other purposes. I HH/tb/0176b . . . . . ' ,. ·---· 1-· ··--... -- : . I -----·-... ----·-··l ◊ FCX Statesville (NCD0954585_27) & Environs--Soil and Groundwater Sample Locations MEMORANDUM TO: THROUGH: FROM: SUBJECT: •• Bill Jeter I Ron McMilla~ / I Jesse W. we11st;w1) :1 FCX P. l.R .F. •• DIVISION OF ENVIRONMENTAL MANAGEMENT February 25, 1986 'GROUND \'/t-TER SECTloti r.ALEIGH. fl.. C. On February 21, 1986, RonjMcMillan, Bill Crawford and I met with Mr. Lonnie Reed, Manager of the FCX Distribution Center in Statesville, North Carolina. Also in attendance ~t this meeting was Mr. Howard Minton, Pesticide Inspector for the Food and Drug Protection Division. This meeting was held in relation to possible ground~ater contamination as a result of repackaging of liquid/dust pesticides. The repackaging of chemicals was ceased in the late 1960' s. ' ,, O.n _,:ebr11ary 8-:9, 1-9,~6, FrJd C. Hart Associates under contract from Southern States Cooperative had four monitor w~lls ··constru~ted on the Fcx· ., . property. Preliminary lab results indicate the presence of nine pesticides (Lindane 55 ppb) in monitor we~l No. 3. No actual lab reports have been submitted to verify the results. I At the meeting, Mr. Reed Jttempted to recall past operational practices which occurred at the plant. ~rior to 1966 liquid pesticides were received at the plant in 55 gallon drums. The pesticides were later repackaged in various sized containers. The !predominant pesticides mentioned were lindane, melathion, chlorodane, inderin, and alderin. Empty barrels were stored on site and later picked up by drum recycling companies. This operation ceased· after opening of the Sumter, S~uth Carolina pl.ant. I I Repackaging of agricultural dust also occurred at the plant. Dust was received in 50 lb. bags and later repackaged. Chemicals predominantly mentioned were DDT, BHC, TDE atid chlorodane dust. After repackaging, the empty dust bags were taken to t:he old Statesville landfill. This operation was ceased in 1969. Mr. Reed also reported that in 1969 he was ordered to bury approximately ' . 5000-10,000 lbs. of DDT, TDE and possibly liquid chlorodane. These products were supposedly buried in their: original containers. The burial depth was reported to be approximately 6 :feet. I have attached a map in the P .I.R.F. report which indicates the appr'oximate location of the burial. Bill Jeter Page Two February 25, 1986 •• Mr. Reed indicated that later Mr. Arch Purcell and Mr. Page Fisher were to meet at the FCX. Mr. PurcJ11 and Mr. Fisher are hired consultants for FCX. A discussion concering the work conducted to present was made. It was agreed that after a written report w~s made available and reviewed from Fred C. Hart Associates that further study will need to be done at the site. ' I I contacted Mr. Phillip Watts, Hydrologist for Fred C. Hart Associates concerning construction permit and well records for the existing monitor wells. He indicated that he would complete the permit application and submit well records. I I • If you should have any qu_est1ons, please advise. JWW:se ? ... ,., i-:· ,... S'!ATCc. ',t/r/{'' ~ 'i ~t, ;,_,a ~I 1t/'53·lrN/J} 'Vr,\'YJ·'.'#Ji)J; ~ North Carolina Department of Human Resources Division of Health Services P.O. Box 2091 • Raleigh, North Carolina 27602-2091 James G. Martin, Governor Phillip J. Kirk, Jr., Secretary Ms. Denise Bland EPA NC CERCLA Project Officer 25 March 19 86 Air and Hazardous Material Division 345 Courtland Street, N.E. Atlanta, GA 30365 SUBJECT: Preliminary Assessment Report FCX NC D095458527 1620 West Front street Statesville, Iredell County, NC Dear Ms, Bland: Ronald H. Levine, M.D., M.P.H. ·, State Health Director Enclosed please find the Preliminary Assessment report for the, subject site. This priority is based on review of available data. FCX Inc. is roughly a 5 acre site located in Statesville, Iredell County, NC. FCX started operations as a distribution center for pesticLdes at this site in about 1940. Prior commercial use of the site is not known •. FCX is now bankrupt. The proposed sale of the site brought to light a reported burial of pesticides on the site. Investigations are underway to deterimine the e~tent of the contamination. FCX recently reported on-site disposal during 1966 of about 5,000 -10,000 pounds of DDT, TDE, and Chlordane. The pesticides were buried about 10' deep. A warehouse with a concrete floor was built covering the area. Other toxic products were handled and may also be on the site. Wastes from "empty" drums may have contaminated other soil on the site. Wastes were taken to the old city landfill. Apparently Southern States authorized investigative engineering studies by Fred c. Hart Assoc. Inc., Washington, DC and four monitoring wells were drilled. subsequently, court ordered studies were continued by Rose and Percell, ?ayetteville, NC. Official reports are not yet available from c, PhiU.p Watts (with F.C. Hart) but a verbal report indicates groundwater contamination in the site wells. The FDA, DEM, Milk commission (Carnation Plant is adjacent to site), and NRCD have been notified. FCX is not a RCRA facility. Ms, Denise Bland Page 2 •• Due to positive indications of substantial amounts of a variety of toxic wastes present on the site it is recommended that soil and water sampling be conducted. Sampling should include the well at the adjacent Carnation Plant and soil samples in the drainage path, A preliminary HRS check indicated that direct contact and groundwater were prime concerns. Based on the available information a Medium priority for inspection is recommended for this site, On 4 March 1986, this Preliminary Assessment was reviewed by CERCLA Unit personnel and by the following representatives from the North Carolina Department of Natural Resources and Community Development, Division of Environmental Management: Fay Sweat, Groundwater Section; Glen Ross, Air Quality Section; and Howard Bryant, Water Quality Section, If you have any questions, please call me at (919) 733-2178, HH/tb/0176b Sincerely, p/~ tP µ✓6. Harry P, Holladay, Environmental Chemist Environmental Health Section Solid and Hazardous Waste Management Branch FAR.· C HA ~ ..... ,. ......... ;··· '!,• C ~; ' . $37.00 --_:_L·· .. . , K Chloranil • . CHEMICAL NAME: 2,3,5,6- TRIVIAL NAME: chloranil. OTHER NAME: Spergon • (I ACTION: Fungicidal seed tre TOXICITY: Acute oral LD5o 1 Chloranil ♦ Chloranocryl -see Dicryl. Chlorasol • -see Ethylene Dichloride. Chlorates Herbicides and defoliants. They act as contact poisons, are trunslocated and may be absorbed from the soil to kill both plant roots and tops. Chlorates cause chlorosis of leaves and a starch depietion in stems and roots when applied in less than lethal doses. See Sodium Chlorate, Magnesium Chlorate. Chlorax • (Product discontinued by Rhone-Poulenc Inc.) CHEMICAL COMPOSITION: Sodium chlorate and sodium meta- borat'!. .\CTION: Weed and grass killer. Chlorazine ♦ (Product discontinued by Ciba-Geigy Corp.) 'CHEMICAL NAME: 2-Chloro-4,6-bis(diethylamino)-s-triazine. ACTION: Herbicide. _ TOXICITY: Acute oral LD~o (rat), 850 mg/kg. Chlorazine • Chlorbenside ♦ (Product discontinued by FBC Limited) CHEMJCAL NAME: p-Chlorobenzylp-chlorophenyl sulfide. CO}.!MON NAME: chlorbemide, chlorsulphacide (Canada). OTHER NAMES: Chlorocide *, Chlorparacide *. ACTION: Acaricide; little insecticidal activity. APPLICATIONS: Used against red spider mites on fruit trees, omamentals, and nursery stock. ?OR~ULATIONS: Wettable powder (20%), emulsifiable cuncentrate (20%). Chlorbenside • Ch!orbicyden -see Alodan •. ('hbrJromuron -see Maloran •. ,_;;:tr:irl:-dam -bee Alicep ·; Alipur •. :.:~1:or Chem T-590 • -see Toxaphene ♦• ,:!,:;rciar. -see Chlordane. Chlordane• • · CHEMICAL COMPOSITION: ical chlordane is a mixture of chlorinated hydrocarbons consistmg of isomers of chlordane and closely related compounds and by-products. About one-half of the composition consists of the two major isomers of chlordane; no other individual component exceeds· about one-tenth of the total product. · . : :. · . CHEMICAL NAME: 1,2,4,5,6,7;'8.8-0ctachlor-2, 3, 3a,4, 7, 7a- hei:ahydro-4, 7-methailoindane. · . COMMON NAME: ~hlordane, chl~rdan .. , OTHER NAMES: Aspon •-chlordane (product discontinued by Faesy & Besthoff), Belt•, Chlor Kil•, Corodane • (PPG Industries), Kj•pchlor •, Niran •, Octachlor •, Octa-Klor, Ortho- Klor •, Synklor •. Topiclor 20 •, Velsicol 1068 •. Also Niran • 5% granular bait. ACTION: Stomach and contact insecticide. CHEMICAL PROPERTIES: Viscous amber-colored liquid insoluble in water but completely miscible in most organic solvents. It is stable toward acid and alkaline conditions that are normally encountered in formulation and application. Vapor pressure is relatively high. TOXICITY: Acute oral LDMI (rat), 367-515 mg/kg; acute dermal (rabbit), > 200 but< 2000 rng/kg. ANTIDOTE: No specific antidote; if swallowed administer emetic of 1 tablespoon mustard in water. SIGNAL WORD: WARNING. CAUTION: Glass or steel containers having a protective baked phenolic coating are used for packing emulsifiable concentrates, water emulsions, and oil solutions. Dusts, dust concentrates, and wettable powders are generally placed in multiwall kraft paper bags. In handling chlordane or its formulations care should be exercised to avoid skin contact, inhalation of dusts or mists, and ingestion. APPLICATIONS: The oil solution type formulation is used almost exclusively for subterranean termite control applications, and emulsifiable con'centrates, granules, dusts, and wettable powders for termite control and certain agricultural purposes. Chlordane has a tolerance of 0.3 ppm on about 50 raw agricultural commodities. FORMULATIONS: Granules, dusts, wettable powders, emulsion concentrates, and oil solutions. Chlordane may be formulated as an emulsifiable concentrate, using any of the usual non-phytotoxic solvents, of which kerosene is most commonly used, and using non- ionic, anionic, and cationic emulsifiers available to the trade. Suitable carriers for use in the manufacture of wettable powder and dust concentrates include diatomaceous earth, fuller's earth, and attapulgite. Inert diluents for dilution or "cutting back" of wettable powder and dust concentrates include kaolin, pyrophyllite and talc. BP: Velsicol Chemical Corp. (Belt•, Octachlor •, Vel- sicol 1008 *) F: Devidayal (Sales) Private Ltd. (India) Tamogan Ltd. (Israel) (Niran *) Chlordecone -see Kepone •. Chlordimeform CHEMICAL NAME: N'-(4-Chloro-o-tolyl)-N,N-dimethyl - formamidine. COMMON NAME: chlordimeform (ANSI, BS!, ISO) (formerly chlorphenamidine). OTHER NAMES: Acaron (discontinued by Schering AG), Bermat •, C 8514, ENT 27567 •, EP-333, Fundal •, Fundex • (discontinued by Schering AG), Galecron *, SN 36268 (Schering AG). Spanone * (discontinued by Schering AG). ACTION: Insecticide-acaricide, ovicide. CHEMICAL PROPERTIES: Buff colored crystals melting at 32° C. Solubility in water, ·250 ppm at 2()) C: dissolves readily in organic solvents. The hydrochloride is soluble in waterto over 50%. TOXICITY: For base: Acute oral LD5o (male rat),.170-220mg/kg; dermal LD5o (rat), 640 mg/kg. Non-toxic to honey bees. For hydrochloride (Fundal • SP): Acute oral LD5o (rat), 325-330 mg/kg; dermal LDMI (rabbit), >4000 mg/kg. Non-toxic to honey bees. For Galecron • 4£ and Fundal • 4E: Acute oral LDM1 (rat), 250 mg/kg; acute dermal LDr.o (rabbit), 2500 mg/kg; acute inhalation LC5o (rat), 3.3 mg/I for 4 hours. Eye irritation (rabbit), severe; skin irritation (rabbit), moderate. SIGNAL WORD: WARNING. ANTIDOTE: Chlordimeform is not a cholinesterase inhibitor. Specific antidote is not known at present. Medical therapy should include usual symptomatic treatment for organochlorine compounds. ' -•.;,..:.1 .... n: .. +: ...... ,. ... , *-Indicates trade name. BP-Basic Producer. F-Formulator. i ; ; -1:: I ; ,I ' !I d . i' I · ); 1: " i :I !, ,, i\ ,, ., ii• ii ,i ·I \1 ' !. I: ' I i I ' d t, 1_.' 1j I 1,. ' i' I 11 i=i ii . Ji ., ,, ,, :i !( ,, I 1\; '. DCPC -see Qikron •. DCPM -see Neotran • and Neosappiran •. 0CU -see Dichloral Urea. • D-D • Soil Fumigant . CHEMICAL COMPOSITION: A 100% mixture of 1,3-dichlo-ropropene, 1,2-dichloropropane, 3,3-dichloropropene, 2,3-dichloropropene, and other related chlorinated hydrocarbons. OTHER NAME: Nemafene •. ACTION: Nematicide. CHEMICAL PROPERTIES: A clear yellow to amber colored liquid, moderately volatile. One U.S. gallon weighs 10 pounds. TOXICITY: Approximate acute oral LDso (rat), 140 mg1kg; (mouse). 300 mg/kg. Acute dermal LDw (rabbit), 2100 mgt kg; inhalation LCw (rat), 1000 ppm (4 hrs). SIGNAL WORD: DANGER. ANTIDOTE: No specific antidote is kno\\'Il. See product label for practical treatment following ingestion, inhalation, or skin or eye contact. HANDLING AND STORAGE CAUTIONS: Flammable. Hazardous by ingestion, inhalation, or by skin absorption. Although toxic to warm-blooded animals, the vapors provide a warning of the presence of D-D •. NIOSH or MESA approved respiratory equipment should be worn when liquid D-D • is exposed to the atmosphere. When handling or working with D-D • wear clean body covering including polyethylene or neoprene gloves and and heavy (grP.ater than 3 mil thickness) polyethylene, neoprene, or rubber footwear; wear eye protection such as chemical workers' goggles. Store in cool place nway from dwellings. Do not cut or weld container. Do not store in or use containers or equipment made of aluminum, magnesiuin, or their alloys. The transP?rtation emergency response identification number is UN 2924. Discarded product is a hazardous waste under RCRA regulations. For further information regarding the safe handling of D-D, please refer to the D-D Handling and Safety Manual. APPLICATIONS: Controlled dosages are injected into the soil where D-D • provides fumigant action against plant parasitic nematodes symphylids, and wireworms on a broad range of crops; also prepla'nt treatment to control bacterial canker and decline of peach trees, for suppression of verticillium wilt, and to control quackgrass in fields to be planted to white potatoes in northwestern _states, fot reduction of damaging effects of verticillium wilt in • ---·•·--· · • . • · ·' r.~ mint production in > aid in control of field i ground. adcast per acre, at least 1g can be done and the of low temperatures or ed at time of planting. 1, Nemex •. ' i(Great Britain) ' ' :etic acid. product of DDT♦• ~ICAL NAME: Dichlorodiphenyldichloroethylene. CHEMICAL PROPERTIES: Product of degradation of DDT+ by !0ss of one molecule of hydrochloric acid (dehydrohalogenation). DDE further degrades to DDA by loss of two more molecules HCl. DDT• HEMICAL NAME: Dichiaro diphenyl trichloroethane. PRINCIPAL ISOMER PRESENT: l.l,l-Trichloro-2,2-bis(p-chlorophenyl) ethnne (not less than 70%). MEDICAL AND PHARMACEUTICAL NAME: Chloropheno-thane. OTHER COMMON NAMES, DDT (BSI. CSA. ESA, ESJ, MAFJ). Zeidane (France), pp' Zeidane. TRADE NAMES: Ano/ex•. Arkotine * (Shell Chemical U.K.}. DDT 35% • (discontinued by Diamond Shamrock de Mexico). DDT Technical. DDT 75% WDP, Dedelo •, Diamekta 50C:C * ·discontinued by Diamond Shamrock de Mexico), Didimar • (ICl). r:Jigmar, Genitox •, ( Gesapon • ,Gesarex "', Gesarol • are obsolete rnde names of Ciba-Geigy Ltd.), Gyron •, Hildit •, Jxodex •, '{opsot•, Micro DDT 75 •, Neocid* (Ciba-Geigy Ltd.), "Jentachlorin •, R50*, Rukseam •, Tech DDT• (discontinued by )inmond Shamrock de Mexico), Zerdane •. 4i¥Ji~H4-Wf& iMw¥fM4U44$ HJSTORi First described .74 by Othmar Zeidler, German chemist, its insecticidal value was not uncovered until 1939 through the work of Paul Miiller in Switzerland. Brought into the United States for testing in September 1942, it was later imported in quantity and by early 1944, domeStiC production for military use was under way. DDT gained rapidly in poPulai-it.Y' be~ause of its very high toxicity to insects, relatively low hazard to warm-blooded animals and due to-the fact that discovery came when rotenone and pyrethrum supplies were very low due to WW Il. Later it was found that DDT is accumulative in the fatty tissue of warm-blooded animals and that special care was required for application to dairy cattle and animals raised for their food value. In further action to prevent con-tamination of food and the environment in general, all uses in the United States except emergency public health uses, and a very few other uses permitted on a case basis, have been canceled as of January l, 1973. ACTION: Insecticide. CHEMICAL PROPERTIES: DDT is extremely non-volatile, almost insoluble in water, has limited solubility in aliphatic oils and is soluble in apolar organic solvents. Crystallization point min. 9()> C; acidity (as sulfuric acid) max. 0.3% in weight; water: Max. 1.0% in weight. DDT· is unstable in the presence of alkalies and therefore is incompatible with alkaloid nicotine and dolomite. Bordeaux mixture, ferbam, and some clays may cause a slight decomposition. TOXICITY: The acute oral toxicity for man has been established at 250 mg/kg. Acute oral LDso (rat), for technical DDT, 113 mg/kg. Toxicity varies widely according to the formulation. Cucurbits, young tomato plants, and beans are injured by normal dosages and DDT may accumulate in the topsoil layer where heavy applications are made annually to crops such as apples. SIGNAL WORD: CAUTION. APPLICATIONS: Build-up of red spider mites often occurs after application of DDT and this plus the fact that a number of major insect pests have shown their capacity to develop a hereditary resistance to DDT has resulted in some displacement by other chemicals. Also used as mosquito vector control for the eradication of malaria in many countries. FORMULATIONS: A contact poison, it is formulated in aerosols, dusts, solutions, wettable powders, emulsifiable concentrates, granular. Space sprays for home use usually are formulated with kerosene and a small amount of methylnaphthalene or xylene to produce 5% solutions. Methylnaphthalene, xylene, cyclohexanone, isophorone, tetralin, or cumene are used as solvents for emulsion concentrates. There is a tendency to cake either before or after grinding so it is often mixed with an equal amount of pyrophyllite or talc before grinding. Addition of a wetting agent to this forms a wettable powder or it can be further diluted and used as a dust. DDT ♦ BP: "Atanor" Sociedad Anomina Mixta (Argentina) Hindustan Insecticides Ltd. (India) (Hildit •, Hildit 50 • WP) Montrose Chemical Corp. of California (DDT Technical, DDT 75% WDPJ Produits Chimiques Ugine Kuhlmann (France) (DDT Technical, DDT 75So WDP) Rumianca S.p.A. (Italy) (DDT 75% WDP and Technical Granular DDT for export; Micro DDT 75 • and R50 •, domestic) Ugimica, · S.A. (Spain) (DDT Technical, DDT 75% WDP) F: All India Medical Corp. (India) (Di,?mar) • Devidayal (Sales) Private Ltd. (India) DDT 35% • -see DDT+ DDT, Antiresistant -see Antiresistant/DDT. DDT Technical -see DDT t. DOT 75 % WDP -see DDT+. DDVF -see DDVP. DC C C p 0 I E D N V A C r. T (r s A HANDLING AND STORAGE CAUTIONS: Do not swallow or get into eyes, on skin, or on clothing. Do-reathe vapors. Not for use or storage in or around home. Do ·ontaminate food or feed products. Keep away from heat and , flame. The transportation emergency response identification number is NA 2783. APPLICATIONS: Used to control certain economically important pests of cotton, soybeans for seed, and ornamentals. Also for coffee borer control. Dicrotophos available for control of elm bark beetles (tree injection system). Enters plant tissue rapidly, thus enabling ;many beneficial insects to survh FOREIGN APPLICATIONS: (Ektafos "). Ciba•Geigy (Swit: Carbicon •; 500 SCW, 1000 SC -:::;;? waterless spraying). .---·--/ Outside U.S., Shell Internation1 g/1 ULV, and lOOOg/1 WSC. FORMULATIONS: 240gramsl ultra-low volume spray. Shell Cl water-miscible product. Bidrin' Dier BP: Ciba'.Geigy Ltd. (S Ektafos ") Shell Chemical Co. (Bidrin "') Shell International Chemical Co. (Great Britain) (Bidrin •) Oicryl • (Product discontinued) CHEMICAL NAME: 3',4'-Dichloro•2-methylacrylanilide. COMMON NAMES: dicryl (WSSA), chloranocryl (BS!, ISO). OTHER NAMES: DCMA, NIA 4556 (FMC). ACTION: Herbicide. TOXICITY: Acute oral LD'" (rat), 3160 mg/kg. APPLICATION: For postemergence use on cotton. FORMULATION: Emulsifiable concentrate (1.6 pounds/gallon). Cl -NHC'Of=CH2 0 CH3 Cl Dicryl • Oicumarol • OTHER NAMES: Dicoumarin •, Melitoxin •. ACTION: Rodenticide. APPLICATION: Superseded by warfarin. Dicuran • -see Chlorotoluron. Didigam • (Product discontinued by ICI Plant Protection Divi-sion) CHEMICAL COMPOSITION: Formulations containing DDT and · lindane. ACTION: Insecticide. TOXICITY: Acute oral LO!,() DDT (rat), 113 mg/kg. Acute oral LD,o lindane (rat), 88 mg/kg. SIGNAL WORD: CAUTION. APPLICATIONS: To control insects destructive to grapes, fodder vegetables, cole crops, clovers; also'rice· Worm, ants, and premise insects." · · · · · FORMULATIONS: Didigam * (20%, DDT, 2% lindane, e.c.), Didigam CJLV• (20%DDT, 2% lindarie, ~y spray). . ~-· ....... J. , .... ,., u..i,u. u,u.1une .I.Uo/o. ACTION: Insecticide. APPLICATIONS: As a replacement for DDT formulations. To control insects d". 'Ctive to grapes, deciduous fruits, potatoes, and ornamentals F: Socit?te po la Protection de !'Agriculture (SOPP.A) (France) Didimac 25 • -see DDT• ; Perenox •. Dieldrex • -see Dieldrin • . Dieldrin • CHEMICAL COMPOSITION: Hexachloro-epoxy-octahydro-endo, exo-dimethanonaphthalene (principal constituent, known as HEOD), with not over 15% related compounds. COMMON NAME: dieldrin (Canada, for pure compound HEOD; Great Britain, Denmark, USSR for pure compound); dieldrine (France). OTHER NAMES: Aluit • (discontinued by Shell International), Dieldrex •, Dieldrite •, Octalox • (Velsicol Chemical), Panoram D-31 ". ACTION: Insecticide. CHEMICAL PROPERTIES: Stable to alkali, mild acids, and to light. Epoxide ring is unusually stable but reacts with anhydrous HBr to give the bromohydrin. Moderately soluble in acetone, soluble in aromatic solvents, insoluble in water. TOXICITY: Acute oral LDIIO (rat), 46 mg/kg; acute dermal LDIIO (rat), 10-102 mg/kg. SIGNAL WORD: WARNING. APPLICATIONS: A contact and stomach poison. It ls usCd for control of soil insects, public health insects, termites, and many other pests. Note: These uses have been canceled in the U.S. FORMULATIONS: Wettable powders, emulsifible concentrates, dusts, granules, seed dressings, solutions. Manufacture discontinued in the U.S. H Cl H Cl Principal constituent of Dieldrin • BP: Shell International Chemical Co. (Great Britain) (Dieldrex •, Dieldrite ") Oieldririe -see Dieldrin • . Dieldrite • -see Dieldrin • . Dienochlor • CHEMICAL NAME: Bis(pentachloro-2,4-cyclopent&dien-1-yl). COMMON NAME: dienochlor. OTHER NAMES: HRS-16, Pentac •. ACTION: Acaricide. CHEMICAL PROPERTIES: Tan crystalline solid; m.p. 122-1230 C; decomposes at 250> C. Insoluble in water; slightly soluble in hot alcohol, aliphatic hydrocarbons, acetone; moderately soluble in aromatic hydrocarbons. . TOXICITY: Acute oral LDoo (rat), 3160 mg/kg; acute dermal LD., (rabbit), greater than 3160 mglkg. Eye irritation (rabbit), slight. Neither a primary irritant nor sensitizer to human skir... ~J_GNAL WORD: CAUTION. · ANTIDOTES: 1f inhaled·, remove to fresh air; if on skin, flush with water and wash exposed areas with soap and water. If in eyes, immediately flush eyes with a directed stream of water for at least 15 minutes. Call a physician. Treatment is symptomatic. Pesticide Dictionary •-Indicates trade name. BP-Basic Producer. F-FOrmulator. ♦-Indicates common name. SLN--Special Local Need. .C95 - ------- 1 ' I ! ! l ,, lignosulfonates (Cont.) ACTION: Dispersants for wettable powders; stabilizers of liquid concentrates. TOXICITY: Relatively nontoxic. Approved as inert ingredients in agricultural formulations by FDA and EPA. APPLICATIONS: Lignosite •, Marasperse • and Norlig • refer to several different types of lignosulfonate dispersing agents suitable for suspending toxicants in the preparation of wettable powders and flowables. Experimentation is usually required to match the proper . dispersant with a specific formulation. These materials are water- soluble, anionic derivatives of lignin. Darvon is a dispersing agent in flowables and wettable dust. Maracell • C will effectively prevent 2,4-D amine concentrates from precipitating when diluted with hard water. Polyfons • are a series of sugar-free sodium lignosulfonate dispersants having varying degrees of sulfonation. Reax • is the name applied to a series of sulfonated lignin dispersants, wetter-dispersants, and metal complexing agents each of which is specifically designed for use in its area of application. All members of the series are sugar-free, highly soluble, free-flowing poWders. Raylig • is the name of a group of sodium lignosulfonates formerly made by ITT Rayonier, Inc. The group consisted of several variations to perform specific functions. See also Lignosol •. BP: American Can Co. (Maracell • C, Marasperse •, Norlig •) Georgia-Pacific Corp. (Lignosite •) Reed Ltd., Chemical Division (Canada) Wy- rough and Loser, Inc .• U.S. ESA (Lignosol •) R.T. V anrlerbilt Co., Inc. (Darvan) Westvaco Corp., Polychemical Dept. (Poly/ans*, Reax *) lihocin * -see Chlormequat C.hloride. Lime -see Hydrated Lime. limestone -see Calcium Carbonate. Lime Sulfur TRIVIAL NAME for an aqueous solution of calcium polysulfides. ACTION: Fungicide; insecticide (scalecide). SIGNAL WORD: CAUTION. Keep out of reach of children. CAUTION: Caustic and disagreeable to apply. Cannot be mixed with soap or oil emulsion without the addition of a stabilizer. May burn when weather becomes warm. HANDLING AND STORAGE CAUTIONS: Causes eye damage and skin irritation. Use waterproof gloves and face shield or goggles when handling concentrate. In case of contact, immediately flush eyes or skin with plenty of w8ter. For eyes, get medical attention. APPLICATIONS: Controls apple scab and powdery mildews by direct action. Provides continued protection by decomposition to leave a residue of sulfur. Largely supplanted by newer synthetic fungicides with a milder action on plants. FORMULATION: Liquid concentrate. BP: Chevron Chemical Co., Ortho Agricultural Chemi- cals Div. Miller Chemical and Fertilizer Corp. Woolfolk Chemical Works, Inc. limit• (Production discontinued) CHEMICAL COMPOSITION: a-Chloro-N,N-diallylacetamide (Randox *) (4 pounds) plus 2,4-D acid (1 pound) per gallon. ACTION: PreemergenCe selective herbicide. APPLICATIONS: For control of certain annual weeds in sugarcane grown in Florida. Also intended to be used on dark heavy soils of the Midwest for field corn, silage corn, and sweet com. See Rando,' (CDAAJ. l.inamex -see Butralin ♦ • lindafor * -see Lindane •· Undagam • -see Lindane ♦• Undagrain • -see Lindane •· lindagranox • -see Lindane ♦• lindal0 • -see Lindane •· linda~ul * -see Lind. ~ CHEMICAL NAME: Gamma isomer of 1,2,3,4,5,6-hexa- chlorocyclohexane. COMl\-1O~ !\AMES: lindane, except Great Britain (gamma BHC, gamma· HCH). OTHER !\AMES: Exagama •, Forlin • (Forshaw Chemicals), Gallogama *, Gamaphex •, Gamma-col •, Gammalin •, Gammex •, Gammexane ·, Inexit •, Lindafor •, Lindagam •, Lindagrain •, Lindagranox •, Lindalo *, Lindamul *, Lindapoudre •., Linda- terra •, Lintox • (Stauffer), Nor;iRam *,Silvano[•. ACTION: Insecticide. CHEMICAL PROPERTIES: Must not contain less than 99.5% of the gamma isomer of BHC. Melting point 112-113°C. Essentially odor-free. TOXICITY: Acute oral LD~ (male rat), 88-125 mg/kg; acute dermal LD:,o (male rat), 1000 mg/kg. SIGNAL WORD: WARNING. ANTIDOTE: Lindane is a central nervous system stimulant for which no specific antidote is available. A short acting barbiturate should be used for alleviation of symptoms. Diazepam is the treatment of choice for convulsions. If ingested, induce emesis, then administer magnesium sulfate and observe. (Some physicians may discourage use of saline emesis.) If on skin, remove contaminated clothing and wash with soap and water; ifin eyes, flush with running water. HANDLI:-IG AND STORAGE CAUTIONS: Store in a dry place. Wear protective equipment to avoid personal contact. APPLICATION: For many uses of which seed treatments are prominent (soil treatment, foliage application on fruit and nut trees, vegetables ornamentals, timber, and wood protection). Possesses more vapor activity than most of. the organochlorine insecticides. FORMULATIONS: Emulsifiable concentrates, wettable powders, oil-base sprays, granules, dusts, aerosols, smoke generator. 40% flowable. Gustafson Flowable Lindane 40%. Recommended as seed tieatment for control of wireworms and seed com maggots on various crops. Currently marketed under SLN registrations. Lacco Hi Lin, 1 pound/gallon lindane used for structural pest control; Lacco Lin-O-Mulsion I. i contains 20% lindane and for use against certain pests of vegetable and horticultural crops; Hog Mange Powder II, Lindane E.C.11 for livestock. COMBINATIONS: See Agrox • 3-Way, Gamatin •, Granol * NM. Duo-Tox • E. C. with toxaphene for livestock. · See gamma-BHC, gamma-HCH. Cl Cl aQc1 Cl Cl 99%gamma OOmer Lindane • BP: Celamerck GmbH & Co. KG (Federal Republic of Germany) (lnexit *) lnquinosa (Spain) Los Angeles Chemical Co. (Lacco Hi Lin, Lacco Lin-O-Mulsion) Rhone-Poulenc (France) (Exagama •, Gallo- gama·•, Gammophele Fog•, Linda/or•, Linda grain •, Lindatranox *, Lindalo *, Lindamul •, Lindapoudre •, Lmdaterra '") Zoecon Corp. F: Devidaval (Sales) Private Ltd. (India) Gustafson, Inc. (Gustafson Flowable Lindane 40%) Hopkins Agricultural Chemical Co. (Lindane E.C.11, Hog Mange Powder II, Duo-Tox • E.C.) ICI Plant Protection Division (Great Britain) (Gamma-col, Gammalin •, Gammexane •) Murphy Chemical Ltd. (Great Britain) lindapoudre • -see Lindane •· liAdaterra • -see Lindane ♦• Lindo! 6G • CHEMICAL COMPOSITION: A formulation (granule! of gamma- BHC (lindane). ACTIO'.\: Insecticide. APPLICATIONS: Recommended for use in lowland rice (Philippines) for control of stem borers (except pink stem borer) and whorl maggot. t I ~ '< ~ 'V 0..l \.I ½ ' , I ~ ~ I 'sS. ·.1 ""' . I'-.,. '-") ~ The Condensed Chemical Dictionary TENTH EDITION Revised hy GESSNER G. HAWLEY ACCEPTABILITY 4 nary ammonium compounds and stances. alkaline sub- (3) A particle accelerator (q.v.). accrptability (foo_ds). See organoleptic. · acceptable risk. A concept that has developed m recent years, especially in connection with toxic substanres (insecticides, mercurials, carcinogens), food additives, air and water pollution, and related environmental concerns. It mav be defined as a level of risk at which a seriously ad~·ersc result is highly unlikely to occur, "but at which one cannor prove whether or nor there is I 00% safety. It means Jiving with reasonable assurance of safety and acceptable uncertainty." {Schmutz, J. F., C&EN, Jan. 16, 1978). Examples of acceptable risk that might be cited are diagnostic x-rays, fluoridation of water, and ingestion of saccharin in normal amounts. Writ,,. Th .. ,.,,.,..,_,_1.:,:h. -• ·'· · ·isks involved in :ome highly con- 1ce appears to be se acetate fiber. gth (psi), 18,000- isture regain 6%; one, acetonitrile, .de, dioxane-1,4. es; beams. nccnaph!hcne ( 1,8-dihydroacena ph thalene; ethyl- enenaphthalene) C10 H6(CH:h. a tricyclic compound. Properties: White needles; sp. gr. 1.024 (99/4°C); freezing point 93.6° C; b.p. 277 .5° C; refractive index ( 1()0° C) !.6048. Soluble in hot alcohol; insoluble in water. Combustible. Derivation: From coal tar. Grades: Technical; 98% Containers: Fiber drums. Hazard: Irritating to eyes and skin. Uses: Dye intermediate; pharmaceuticals; insecticide; fungicide; plastics. acen~phthcnequinone ( 1,2-acenaptbenedione) C10H0(CO)i. a tricyclic compound. Properties: Yellow needles: m.p. 261-263°C; insol- uble in water; soluble in alcohol. Derivation: By oxidizing acenaphthene, using glacial acetic acid an<l sodium or potassium dichromate. Grades: Technical. Uses: Dye synthesis. s.ccnocoumarin ( 3-( a I pha-aceton yl-4-ni t robenzy 1)-4- h yd rox ycou ma ri n) C19H 15!\'O~. Properties: White crystalline powder, tasteless and odorless; m.p. 197°C. Slightly soluble in water and organic solvents. Low toxicitv. Use: Medicine (anticoagulant): • accphatc (accty!phbsphoramidothioic acid ester) C,H10NO3PS Properties: White crystals; m.p. 65°C; soluble in water; slightly soluble in acetone and alcohol. Hazard: Moderately toxic by ingestion. Use: Insecticide. acctal (diethylacetal; l, 1-diethoxyethane; ethylidenedi- cthyl ether) CH3CH(OC,H,)1• Properties: Colorless, volatile liquid; agreeable odor; nutty after•iaste. Stable to alkalies but readilv decomposed by dilute acids. Forms a constant. boiling mixture with ethyl alcohol. Soluble in alcohol, ether, and water. Sp. gr. 0.831; b.p. 103- 1040C; vapor pressure 20.0 mm (20°C); flash point (closed cup) -5° F (-20.5° C); specific heat 0.520; refractive index 1.38193 (20°C); wt (lb/gal) 6.89; autoignition temp. 446° F (230° C). Derivation: Partial o.xidation of cthvl alcohol the acetaldehyde first formed conden.sing with. the alcohol. Grades: Technical. Containers: Cans; carboys. H:irnrd: Highly flammable. Dangerous fire risk. Explosive limits in air 1.65 to 10.4%. Moderatelv toxic and narcotic in high concentrations.. • Uses: Solvent; cosmetics; organic synthesis; per- fumes; flavors. Shipping regulations. (Rail,_ Air) Flammable Liquid label. See also acetal resin. 11cetaldehyde (acetic aldehyde; aldehyde; ethanal; ethyl aldehyde) CH,CHO. Properties: Colorless liquid; pungeni, fruity odor. Sp. gr. 0. 783 ( 18/ 4°C); b.p. 20.2°C; m.p. -123.l°C; vapor pressure 740.0 mm (20°C); flash point -40°F (-40°C) (open cup); specific heat 0.650; refractive index l .3316 (20°C); wt. 6.50 lb/gal (20°C); miscible with water, alcohol, ether, benzene, gasoline, sol• vent naphtha, toluene, xy\l':ne, turpentine and acetone. Derivation: (a) oxidation of ethylene; (b) vapor- phase oxidation of ethanol; (c) vapor-phase oxi- dation of propane and butane; (d) catalytic reaction of acetylene and water (chiefly in Germany). Grades: Technical 99%. Containers: Steel drums; tank cars. Hazard: Highly Oammablc; toxic (narcotic). Danger- ous fire and explosion risk. Explosive limits in air 4 to 57%. Tolerance, JOO ppm in air. Uses: Manufacture of acetic acid and acetic anhv• dride. n-butanol. 2-cthylhexanol. peracetic acid, aldol, pentaerythrito!, pyridines, chloral, 1,3-butvl- ene glycol, and trimcthylolpropane: synthe~ic flavors. Shipping regulations: .(Rail. Air) Fl2.mmable Liquid label. Not acceptable passenger. acctaldchydc ammonia, Sec aldehyde ammonia. acctaldehydc eyanohydrin. Sec lactonitrile. ~;(-~~'f'r-r.-... ....,_ . . "r.~•·rn -.-"'· ., . ~•or,,...... . ,.~:•:"'-'lJl"!'~ ' ., · ·CS·"'""'"'"'"""' m'.··""'""' ,rr:,cc..,,.===~ --~; .·•-,,,. )>;, .;: _:-· ,· \::.~ >{; ~,, ,,. -;~, '. acctaldol. See aldo\. acrtal resin (po!yacetal). A I plastic polymer obtained b• mcrization of formaldch· linear molecule of the type Sing!e molecules mav hav As the molecule ha; nos arc formed. Acetal resin wugh and resilient; die!ect strength 1200 volts/mil (2 mil); dimensionally stable ture and heat, rcsistan1 flexing and creep, and h; friction surface. Can be ch molded. extruded, and b mended for use in strong a be homopolymers or cope Properties: Sp. gr.· 1.425; t Btu/ hr/ sq ft/° F / ft; coeffii 4.5 X 10·5 per ° F; speciJ water absorption 0.41 % 10,000 psi; elongation I'. R 120; impact strength (n, ural strength 14,100 psi; Combus1ible, but slow b11 Uses: An engineering plasti for metals, as oi! and g~ appliance parts; industri: munication equipment; cosmetics. See also "Delrin"; "Ce!con aeetamidc (acetic acid ami CH,CONII,. Properties: Colorless de\ic odor. Soluble in water an, in ether. Sp. gr. 1.159; refractive index 1.4274 (7 Derivation: Interaction of nium hvdroxidc Grades:· Technic~l; C.P. reagent. Containers: Fiber cartons. Hazard: Has caused cancer Otherwise low toxicity. Uses: Organic synthesis (r~ stabilizer); general so!Ye soldering flux: hygroscoJ penetrating agent. acetamidine hydrochloride Properties: Crystalline sol m.p. I 66° C: soluble in wa in acetone. Keep stoppere Derivation: Alcohol sol HCI + ammonia. Hazard: Skin irritant. Mod Use: Synthesis of pyrimidi1 biochemically acti\'e comr acetarnido-. Prefix indicati1 Also called acctamino-or Uses: Compounding of brighteners requiring a uni- form dry solid bisulfite c0mplex for electroplating. AI\'PO. Abbreviation for alpha-naphthylphenyl- oxazole. "Anstac-2M:'m Trademark for an antistatic and cieaning agent for plastics, such as methyl meth-acrylates, vinyls, and polystyrenes. Containers: l-qt bottles; 1-, 5-gal drums. Uses: In aircraft, sign, novelty, electrical, photo- grJphic, optical, and other industries. antacid. Any mildly alkaline substance, such as sodium bicarbonate, taken internally in v.'ater solu-tion to neutralize excess stomach acidity. antagonist, structural (antimetabolite). An organic compound that is structurally related to a biologi-cally active substance (enzyme, nucleic acid, amino acid, etc.) and which acts as an inhibitor of its growth and development. Such biological antag- onism exists between sulfa drugs and p-amino- benrnic acids, and also between histamine and a group of compounds collectively called anti.hista- mines (q.v.). One of the most important of these from an agricultural standpoint is imidazole (q.v.) which, together with similar compounds, is used to "antagonize" the metabolism of insects, especially those attacking fabrics: it is also being used in irriga- tion waters to protect plants from deleterious pests. Structural antagonists have important medical applications in the complex field of allergic disease. See also chemotherapy~ antigen-antibody. ''Anta.on FC-34."~01 Trademark for a high foam- ing, water soluble, amphoteric surfactant with soap~like qu<tlitic!.; a complex fatty amido com- pound; 40% active. Uses: Fulling agent and detergent for woolen and worsted fabrics, effective under neutral, acid and alkaline conditions; recommended for use in bubble baths, detergents; in soaps for dedusting purposes. "Antarox.''w1 Trademark for a series of surfactants. Uses: Viscose spin bath additive, preventing accumu-lation of sludge in pipe lines, reels, etc.; prevents clogging of spinnerets; in manufacture of cello- phane, prevents deposits from forming on extrusion slits and rollers; in the steel industry, to obtain cleaner sheets in the final wash of the reduced sheet during cold reduction. antarnline CliH1~NJ. Properties: White. odorless crystalline powder with bitter taste. M.p. l20°C. Sparingly soluble in alcohol and water; practically insoluble in benzene 2nd ether. Hazard: The phosphate is toxic. Use: Medicine (aniihistamine). Available as hydro-chloride and phosphate. anteiso-. Prefix denoting an isomer (usually a fatty acid or derivative) which has a single, simple branching attached at the third carbon from the end 75 1.8.9-ANTHRACENETR!OL of a straight chain, in distinction to an iso-com- pound, where the attachmrnt is to the second carbon from the end. For example, isododecanoic acid would be CH,Cll(CH,)(CH2).COOH, while anteisododecanoic acid would be CH,CH,CH(CH3)(CH,),COOH. anthelmintic. An agent used in veterinary medicine as a vermifuge. anthelmycin. USAN' name for an antibiotic sub- stance produced by Streptomyces longissimus. anthocyanin. A flavonoid plant pigment which accounts for most of the red, pink, and blue colors in plants, fruits and flowers. Water-soluble. See also flavonoid. "Anthomine."300 Trademark for a dying assistant primarily for use in wool dyeing. .anthopyllite (Mg,Fe)7Si801:(0H)2• A natural mag-nesiu ~· _ _s_jlicate. See asbestos. -,.,•~n!,!t!!h!.'rac,c"'e~n~e _,C"'ee;H!.''Cl:C"'-!.llu;.c• ,.....::> Properties: Yellow crystals with blue fluorescence. Soluble in alcohol and ether; insoluble in water. Sp. gr. 1.25 (27/4°C); m.p. 217'C; b.p. 340°C;Oash point 250°F (!2l0 C) (closed cup). Combustible. It has semiconducting properties. Derivation: (a) By salting out from crude anthracene oil, and draining. The crude salts are purified by pressing and fina!ly, by the use of various solvents, phenanthrene and carbazole are removed~ (b) by disti!ling crude anthracene oil with alkali carbonate in iron retorts, the distillate containing only anthra- cene and phenanthrene. The latter is removed by carbon disulfide. Method of purification: By sublimation with super- heated steam, or by crystallization from benzene followed by sublimation; for very pure crystals, by zone melting of solid anthracene. Impurities: Phenanthrene, carbazole and chrysene. Grades: Commercial (90 to 95%); pure crystals. Hazard: A known carcinogen. Uses·. Dyes; alirnrin; phenanthrenc; carbazo!e; anthraquinone; calico printing; as component of smoke screens; as scintillation counter crystals; organic semiconductor research. flnthracenc oil. A coal~tar fraction boiling in the range 270-360°C; a source of anthracene and similar aromatics. Also used as a wood preservative. and pesticide, except on food crops. Ha1.ard: A known carcinogen. 1,8,9-.anthr.accnctriol. See anthralin. ' / I j 251 CHYMOSIN HO,sco 1 ~ 50,H ::::::.._g 1# BO OH Properties; \\'hite needles; soluble in water; insoluble in alcohol and ether. Derivation: Reaction of H-acid with JO% NaOH at 280, c. Uses: Azo dye intermediate; analytical reagent. chromous bromide (chromium bromide) CrBr2. Propcrti~s: White crystals; changes to yellow on heating. Oxidizes in moist air but stable in dry air. Sp. gr. 4.356; m.p. 842°C; soluble in water (blue color). Hazard: Toxic by ingestion; irritant to skin and tissac. Tolerance (as Cr), 0.5 mg per cubic meter in air. chromous ecrbonate (chromium carbonate) CrCO3. Properties: Grayish-blue amorphous mass; sp. gr. 2. 75. Soluble in mineral acids; slightly soluble in water containing carbon dioxide; insoluble in al- cohol. Hazard: Toxic by ingestion; irritant to skin and tissue. Tolerance (as Cr), 0.5 mg per cubic meter in air. chromous chloride (chromium chloride) CrCb. Propt:rties: White, deliquescent needles; sp. gr. 2.878 (25°C); m.p. 824°C; active reducing agent; very soluble in water; insoluble in alcohol and ether. Derivation: Reaction of the metal with anhydrous hydrogen chloride. Hazard: Toxic. Tolerance (as Cr), 0.5 mg per cubic meter in air. Uses:·Reducing agent; catalyst; reagent; chromizing. chromous oxalutc CrCiO,· HiO. Properties: Yellow crystalline powder; sp. gr. 2.468; solub!e in water; active reducing agent. Hazar'd: Toxic by ingestion; irritant to skin and tissue. Tolerance (as Cr), 0.5 mg per cubic meter in air . .. Chromoxane."307 Trademark of mordant dyestuffs. Used on wool; characterized by fairly good fastness to light, very good fastness to fulling, etc., and by relatively bright shade. "Chromspun."n6 Trademark for a solution-dyed ace• tate fiber. chrom~·I chloride (chromium oxych\oride; ch!oro- chromic anhydride) CrO:::Ch. Properties: Mobile, dark•red liquid. B.p. I 16°C; freezing point-96.5°C; sp. gr. 1.911. Fumes in air; reacts ,·igorously with water to form chromic acid, chromic chloride, hvdro,::hloric acid, and chlorine. Miscible with carb.on tetrachloride, tctrachloro• ethane, carbon disulfide. N'onconductor of eke• tricity. Strong oxidizing agent. Protect from light and moisture. Deri\'<ltion: By heating sodium dichromatc and so• dium chloride with sulfuric acid. Hazard: Toxic. Corrosive to tissue. Uses; Organic oxidations and chlorinations: solvent for chromic anhydride; chromium complexes and dyes; catalyst. Shipping regulations: (Rail, Air) Corrosive label. ~ at acceptable passenger. chromyl nuoride (chromium o.xyfluoride) CrF1O1. Properties: Black crystals; sublimes at 29.6° C; poly· merizes on exposure to light. Hazard: Highly reactive; ignites hydrocarbon gases at high temperatures. Toxic. Uses: Fluorination catalyst; dyeing polyoldins. chrysamine G C16H16r-..1.O6;-,fa2. Properties: Yellowish•brown powder. Very sparingly soluble in water. Derivati, salicylic Use: Yer chrysanth (CH,),< Properti ester oc in watc Contain Haza;d: Uses: S~ icides; Sec a!s< ciuysazi1 chrysene ( l.2•benzphenanthrene) C1s H11 (a tetra• cyclic hydrocarbon) Properties: Crystals; sp. gr. l.274 (20/4°C); m.p. 254°C; b.p. 448°C; sublimes easily in a vacuum. Slightly solu blc in alcohol. ether, glacial acetic acid. Insoluble in water. Derivation: Distillation of coal tar. Hazard: Carcinogenic agent. Toxic. Use: Organic synthesis. chr,·soidine hydrochloride (meta•diaminoa1.oben• zene hydrochloride} (C6 H,N?--:C6 H3(NH2)i· HCI. Properties: Red-brown powder or large black shiny crystals with a green luster. Soluble in alcohol and water giving orange•brown solutions. Insoluble in ether; m.p. l J 7° C. Uses: Orange dye for cotlon and silk. chrysolite. See olivine. chrysotile. See .1sbestos. chu. Abbreviation for centigrade heat unit. It is the amount ofhi::at required to raise the temperature of one pound of water one centigrade degree from 15° C to I 6° C. It is sometimes called a pcu (pound centigrade unit). chymosin. See rennin. 'I ! ,' •.' 2 341 pressure 0.58 mm (200°C); insoluble in water; \'iS-cosity 26.3 cp (20°C). Flash point 425°F (218°C). Combustible. Low toxicity. v~e: rtasiicizer. di<lecylnmine [CH1(CH,)?]2NH. Propenies: Light straw-colored liquid; faint amme odor: boiling range l95-215°C ()2 mm); sp. gr. 0.840 (20/20°C) (solid). Combustible. didecyl ether (C1uH21).;0. Properties: Liquid; m.p. 16°C; b.p. 170-!80°C (6 mm); sp. gr. 0.819 (20/4°C); refractive index 1.4418 (n 20/ D). Combustible. Grades: 95% (min} purity. · Uses: Electrical insulators; water repellent; !ubricant in plastic molding and processing; antistatic agent; intermediate. didcc)·I phth•late (DDP) C.11,(COOC,olli,):. Properties: Light-colored liquid: sp. gr. 0.9675 (20/ 20' C); 8. 05 lb/ gal (20°C); b.p. 261 ° C (5 mm); in sol• ublc in water; vapor pressure 0,3 mm Hg (200°CJ: viscosity 113, 2 cp (20°C); nash point 445° F (229°C). Combustible. Low toxicity. Containers: Drums, tank cars; tank trucks. Use: Plasticizer, especially for vinyl resins. rlitiec,rl sulfide (didecyl thioether) (CioHnhS. Properties: Liquid; solidifies at 22.2°C; b.p. 205-2060C (4 mm); sp. gr. 0.831 (20/4°C); refractive index 1.4569 (n 33.5°C/ D). Combustible. Grades: 95% (min.) purity. . Use: Organic synthesis (formation of sulfonium com~ pour.ds). didecJl thioether. didodecylamine. didodecyl e1hcr. Sec didecyl sulfide. See dilaurylamine. See dtlauryl ether. did odecyl-3,3 '•thi od i propionate. di propionate. See di!auryl thio- didorlecyl lhioether. See dilauryl sulfide. DIOP, See diisodecyl phthalate. didymiurn Di Commercial mixture of rare earth e!ements ob-tained from mona1.ite sand by extraction followed by the elimination of cerium and thorium. The name ls used like tha:. of an element in naming mixed ox-id1:s and salts, The approximate composition of didymium from mona1.ite, expn:ssed as rare earth oxides is 46% lamhana, La~O3; 10% praseodymia, Pr60:t; 32% ncodyrnia, Nd:,O3; 5%samaria, Sm.;O3; 0.49t yttrium earth oxides; 1 % ceria, CcO;; 3% gadolinia Gd~O3; 2% others. Commercially used didymium salts are acetate, carbonate, chloride, fluoride, nitrate, etc. Didymium oxide; Di;O3; brown powder; insoluble in water; soluble in acids. Containers: Glass bottles; fiber and steel drums. Uses (as r,ahs): Coloring and decolori1.ing glass; in tt:mpcraiure-compensaiing capacitors for radio, "'•~ .•. ' ~:t~: 'r; .. :f -·~~ r1-::, -•:ii •, ·~7 t-; ..... ...:,•:.. DIELECTRIC television, and radar; in carbon arc cores (fluoride); in stainless steel ( oxide): metallurgical research; tex-tile treatment. Shipping regu!ati.ons: direr label. (didymlum nitrate) (Air) Oxi• die. A device, usually of steel, having a specific shape or design, which it imparts to such materials as metals and plastics, either by impact (stamping), by the contour of a negative cavity (casting), or by passing the material through it (extrusion). Dia-mond dies may be used for wire-drawing. The terms "die" and "mold" are virtually synonymous in the sense of a negative cavity into which a mo!ten metal or plastic is introduced under pressure, the former bci,ng used in reference to metals and the }alter for plastics, rubber. etc. See also die castim?: investment casting; inject die casting. St molten metal negative-cavit The die is us commonly us, copper, lead , include silico ances as low 75 to !00 lb end-use area: plane parts; t} machines, ele for various rr I dieldrin (HEOD) C1,;HioOCk Generic narne for an insecticidal product containing not less than 85% of 1,2,3,4, I 0, l O -hexachloro -6, 7 -epoxy -1 ,4,-fa,5,6,-7 ,8,8a -octahydro-l ,4-endo,exo-5,8 -dimethano-naphthalcne, and not less rhan 15% active related compounds, See also endrin, a stereoisomer of dieldrin. Properties: LighHan, f1aked solid, m.p. 175°C. In-soluble in water, methanol, aliphatic hydrocarbons; soluble in acetone, benzene. Compatible with most fertili1.ers, herbicides, fungicides and insecticides. Derivation: By oxidation of aldrin (q.v.) with per-acids. Containers: fiber drums. Hazard: Highly toxic by ingestion, inhalation and skin absorption. Penetrates intact skin. Tolerance, 0.25 milligram per cubic meter of air. Use restricted to ~onagricu!tural applications. Said to be carcino-genic. Use: Insecticide. Shipping regulations: !'\o label required. dielectric., A substance that has verv low electrical conducti\'ity, i.e., an insulator_ S~ch substances have electrical conductivity of less than 1.000,000th rnho per cm. Those with a somewhat higher conduc-tivity ( !0-6 to !0-3 mho per cm) are called semicon-ductors (q,v.). Among the more common solid dielectrics are glass, iubber and similar elaslomers, wood and other cellulosics, Liquid dielectrics are I ' ,!' I of classical mechanics. Sec also liquid, l\'cwtonian; rheology; fluidization; hydraulic fluid. fluid hc-d. See fluidiwtion. fluidization. A technique in which a finely divided solid is caused to behave like a fluid by suspending it in a moving gas or liquid. The solids so treated are frequently catalysts; hence, the term fluid catalysis. The fluidized catalyst. e.g., alumina-silica gel, is brought into intimate contact with the suspending liquid or gas mixture, usually a petroleum fraction. Loc:al overheating of the catalyst is greatly reduced, and portions of catalyst can be easily removed for regeneration without shutting down the unit. There arc also non-catalytic applications of f1uidization, e.g., reduction of iron ore. Important uses of the fl:iidized bed process are (1) cracking of petroleum fractions: (2) gasification of coal; (3) application of organic coatings to metals (fusion bond method); (4) Coal combustion, in which sulfur-bearing coal ( ll in. diameter) is fed into a fluidized bed of limestone. Combustion occurs at 16000 F, at which temperature the limestone is reduced to lime, which reacts with the sulfor in the coal to form gypsum. This technique makes possible the use of high-sulfur coal without necessity of scrubbers. The bed material is about 5% coal and 95% limestone products. fl•rnboric acid (fluoroboric acid) HBF4. Properti~s: Colorless, strongly acid liquid; sp. gr. approx l.84;b.p.130C with decomposition. Miscible with water, alcohol. Dcivation: Action of boric and sulfuric acids on nuor:.par. Grades: Technical (about 48%); pure. Hazard: Highly toxic; a corrosive irritant. Uses: Production of fluoborates; electrolytic bright-ening of aluminum; throwing power aid in electro-lytic plating baths; esterfication catalyst; metal cleaning; making stabilized diazo salts. Shipping regulations: (Rail, Air) Corrosive label. "Fluokarb."1s4 Trad cm ark for an activated bonechar used for f1uoride removal. flu or. See phosphor. fluophosphalc rhosphatc. fluoranthene carbon. alkyl ester. Sec diisopropyl fluoro- Pruperties: Co!Ol'ed needles: f.p. 107°C: b.p. 250°C \(.0 mm); insoluble in water: soluble in ether and benzene. Combustible. Derivation: From coal tar. Hanrd: Moderately toxic. Oucrnpatite. See apatite. nuor bensidr. Generic name accepted for para-chloro~ benzyl para-fluorophcnyl sulfide, ClCd·fJCJ-hSC~lt F. Crystals; m.p. 36° C. Insoluble in water; soluble in ncetone and oils. Used as an acaricide. "Fluore/"158 Trademark for a fully-saturated fluo-rinated polymer containing more than 60 per cent Ouorine by weighl; non-Oammable. Uses: 0-rings, gaskets; hoses: wire and fabric coatings; diaphragms; fuel cells; expcllent bladders; sealants; insulation; containers. fluorene ( a I pha-d i phen ylenemet ha ne} ~--~ C6H~C~hC,H4. A tricylic hydrocarbon. Properties: Small, white, crystalline plates; fluores-cent when impure. Soluble in a]coho!, ether, benzene and carbon disulfide; insoluble in water. M.p. 116° C; b.p. 295° C (with decomposition). Combus- tible. Derivation: By reduction of diphenylene ketone with zinc; from coal tU:r. Grades: Technical; 98% pure. Uses: Resinous products; dyestuffs. fluorescein (resorcino!phtha!ei n; diresorcinolphtha- lein; see also urar.ir,e) C20 H1c05• C.I. 45350 Properties: Orange-red, crystalline powder; very dilute alkaline solutions exhibit intense, greenish-yellow fluorescence by reflected light, while the solution is reddish~orange by transmitted light; m.p., decom-poses at 290°C; soluble in dilute alkalies, boiling alcohol, ether and dilute acids, glacial acetic acid; insoluble in water, benzene, chloroform. Combus-tible; low toxicity. Derivation: By heating phtha!ic anhydride and resor-cinol. Grades: The sodium salt {uranine) and potassium salt are marketed. Uses: Dyeing sea water for spotting purposes; tracer to locate impurities in wells; dyeing silk and wool; diagnostic aid in ophthalmolo.i;y; indicator and reagent for bromine. nuore~ccnce. A type of luminescence (q.v.) in which an atom or molecule emits visible radiation in n, passing f ram a higher to a lower electronic state. The term is restricted to phenomena in which the time interval between absorption and emission ofenefgy is extremely short (JO-to 10-3 second). This distin- guishes fluorescence from phosphorescence, in which •L-•=-n :~,,. .. ,,,,,1 rn~v r.xtend to several hours. ,lid, organic 1 as zinc or 5, television ilar devices. nolccules in horescence: g water sup- salt for the ental caries. r city fluori- dium silica- -~~ '•'h '0-;>~ "" ... i r·!' "P\IANTOUD" pH control is of critical importance in a large number of industrial operations such as water purification. chrome tanning process for leather. in preservation of food products. in electroplating baths. dyeing, agriculture, and numerous other instances. See also acid; base. 794 "Phant~lid.''105 Trademark for a standardized mix- ture of structural isomers of I, 1.2,3,3,5-hexamcthyl- indan methyl ketone. Properti,;::;.: \Vaxy. white solid w:th musk-like odor that begins to sinter at about 35°C and becomes liquid at about 40° C. Soluble in conventional solvents and essential oils. Use: Perfumery. pharmaceutical. A bro;)d term that includes not only a\l types of drugs. medicinal and curative products but also ancillary products as tonics, dietary supple- ments, \'itamins, deodorants and the like. Sec also drug. phase. ( 1) One of the three states or conditions in which substances can exist, i.e .. sohd, liquid. or gas(va por). The condition depends primarily on the concentra- tion of atoms or molecules: solids are the most dense, gases the least, and liquids occupy the intermediate position. Solids are normally crystal- line, liquids are amorphous, and gases are without structure. See also matter. (2) A physically distinct and mechanica\ly separa- ble portion of a dispersion or solution. Phases may be either solid. liquid. or gaseous (vapor). In any mixture or solution the major component is ca\\ed the continuous or external phase and the minor component the dispersed or internal phase. The latter may or may not be uniformly dispersed in the continuous phase. See colloid chemistry; solution. phase rule. Propounded by J. Willard Gibbs (q. v.) in 1877, the phase rule isa general system F = n-r-2 stating the boundaries of thermodynamic equilib- rium in a system of chemical reactants. The number of degrees of freedom (F) allowed in a given heterogene< or observat choice ofth independen presrnre. Tl multicompc glas~: alloy! Phe Abbrev alpha-phellam h~xadiene) 1 A monocyc /-optical iso Properties: ( in ether. (a) mm): rcfra1 (20°C); b.p. 58-59°C (!6 mm); refractive index 1.4724. Combustible. Derivation: (a) Found in ginger oil; Ceylon and Seychelles cinnamon oil. (h) Found in eucalyptus oil. Hazard: Moderately toxic by ingestion and skin absorption; strong irritant. Uses: Flavoring; perfumery. bern-phe 11:rndrene ( 4-isopropy\-1-met hylene-2-cyclo- hc xc ne) CH,: CCH: CHCH[ CH(CH,),]CH,CH,. A monocyclic terpene occurring as (a) d-and (b) /-optical isomers. Properties: (a) Mobile oil with pleasant odor and a burning taste. Sp. gr. 0.8520 (20° C); b. p. 171-172° C (760 mm); refractive index 1.4788. (b) Mobile oil; sp. gr. 0.8497 ( 15' C); b.p. 178-179'; nash point 120' F (48.9' C) (T.C.C.). Refractive index I :4800. Both are insoluble in water and alcohol; soluble in ether. Combustible. phenacainc hydrochloride C,H,OC,H,NCH(CH,)NC, H,OC,H,· HCI· H,O. N ,N '-Bis(pa ra-et hoxyphenyl)acetamid ine h ydroc hlo- ridc. Properties: Sma\\, white crystals; odorless; faintly bittcrtas1e. lncompatiblcwithalkalies. M.p.190°C. Soluble in alcohol, boiling water and chloroform; less so in cold water, insoluble in ether. Grades: N.F.; technical. Hii."zard: Toxic by ingestion. Use: Medicine (topical anesthetic) phenacetin. U.S. P. name for acctophenetidin (q. v.). phcnacyl chloride. See ch\oroacetophenone. phcnacyl fluoride. See f1uoroacetophenone. phenanthraquinone. See phenanthrenequinone. phcnanthrene C1,H10. CK] Properties: Colorless, shining crystals. Soluble in alcohol, ether. benzene, carbon disulfide and acetic acid; insoluble in water. Sp. gr. 1.063; m.p. 100.35°(; b.p. 340° C. Combustible. Derivation: Fractional distillation of high-boiling coal-tar oils. with subsequenl recrystallization from alcohol. Hazard: Toxic. A known carcinogen. Tolerance .02 mg per cu meter of air. Uses: Dyestuffs: explosi\'es: synthesis of drugs; bio- chemical research; phenanthrenequinone. phenanthrcn(·quinone. (Erroneously: phenanthraqni- none.) C1,l-hO!. Properties: Yell ow-orange, needle-like crystais. Solu- ble in sulforic acid, bem.:ene; glacial acetic acid and hot alcohol; insoluble ir 206-207'C; b.p. subl Derivation: By oxide phenanthrene in g!3 acid, solution in sod means of hydrochlo, Uses: Organic synthes 1,10-phenanthroline ( nanthroline) C12 H~?'- pound. Properties: White cry: anhydrous l 17°C. S in alcohol, benzene, Deri,·ation: Heating glycerol, nitrobenzc acid; also from 8-arr Uses: Forms a compl1 used as an indicator phenarsazine chloride. sine. phenazine (azophen) compound. Properties: Yellow er 360° C; very slight soluble in alcohol a1 Uses: Organic synth1 vicide. phencthieillin. penicillin. See I phcnethyl arctale. S( phenelhyl alcohol (pt no!; benzyl carbinol Properties: Colorless ing taste; sp. gr. 1.0 I (n 20/D) 1.5310-1. Flashpoint216°F( soluble I part in 50 oils, alcohol, and glJ oil. Combustible. Derivation: (a) By r ester by sodium in action of ethylene o mide and subsequer many essential oils. Grades: Technical;;-.:, Containers: Tin cans Uses: Organic svnth flavors; antibac~eri:-i sec-phenethyl alcohol hol. phcnethylamine. Se1 phenethyl anthranilal 1n te. phenethyl isobut)·ra· tyrate. P\'RAZOLINE 872 Hazard: To:xic by inges1ion and inhalation; irritant to skin anJ eyes. Uses: Chemical intermediate; stabilizer for haloge- nated solvents and lubricating oils. pyraioline H;,-.:~CHCH,Cl·b. B.p. 144°C. Use: Organic synthesis. pyrnrnlonc dy'!. A dye whose molecules contain both the-~='\'-and the =C=C= chromophore groups in their structure. These are acid dyes most used for silk and wool, and to some extent for lakes. Tartrazine. C.L 19140. is an important member of this group. Sec dye. ''Pyre•M. L.''16 Trademark for polyimide coated fa b- rics and la minatcs; used as class H c\cctrica! insulat- ing materials.· pyrcne C1bH\O. A condensed ring hydrocarbon. Propc:-tics: Colorless solid (tetracene impurities give :i yellow color); solutiO;"tS have a slight blue nuores- cencc. M .p. I 56° C: sp. gr. 1.271 (23° C); b. p. 404° C. Insoluble in water: partially soluble in organic solvents. Derivation: From coal tar. Hazard: A c::1r~inogcnic agent. Absorbed by skin. Use: Biochemical research. "'"r ofchrysan- •tent insecti- s. Sec also 1dily in air. immon sol- ;1.nd inha\a- ·ocs, garden :>r shipping of chrysa n- ur primary 1m nowcrs. ____ J-'.''~"""' 1, c11li:nn I and II. Properties sirnibr to those of pyrethrin I. pyrethrum. A natura I insecticide obtained by extrac- tion of chrysanthemum flowers native to Kenya, Ecuador and Japan. The solvent used is a hydro- carbo;i of the kerosine 1ype. Pyrethrum is a!so made synthetically. Not compatible with alkaline material. The chief constituents are pyrethrins I and II and cinerins I and II (see also al!ethrin). These com- pounds are nonvolatile and very slightly soluble in water. Hazard: Toxic hy inges1ion and inhalation. Tolerance, 5 mg per cubic meter of air. Uses: Hou.sehold insecticide (flies, mosquitoes. garden insects, etc.). "P)·rcx Glass Brand ;";a. 7740.''20 Trademark for a borosilic::tte glass. Properties: Linear cocfficienl of expansion, 32 X I0-1 J°C; elasticity coefficient 6.230 kg/sq mm; hardness (scleroscopc) 120; sp. gr. 2.25; specific heat 0.20: refractive index 1.4 74 dispersion 0.00738; light and heat transmission higher than the best plate g!ass; dielectric constant 4.5 (25° C): upper working temperature (mechanical considerations only): an- nealed, extreme limit 490° C, normal service 230,:, C; thermal stress resistance 53°C; impact abrasion resistance 3.1; softening temp. 8200C. Uses: l..abMatory and pharmaceutical glassware and apparatus; electrochemical equipment; fiber manu- facture; domestic ovenware apparatus and equip- ment for many processes. pyridine N(CH),CH. Properties: Slightly yellow or colorless liquid; na useat- ing odor; burning taste; slightly alkaline in reaction. Soluble in water, alcohol, ether, benzene, ligroin and fatty oils. Sp. gr. 0.987; f.p. -42.0°C; b.p. 115.5°C; flash point (closed cup) 68°F (20"C). Autoignition temp. 9000 F (482:>C). Derivation: (a) By coal carbonization, and recovery both from coke-oven gases and the coal tar middle oil. (b) Also synthetica!:y from acetaldchyde and ammonia. Grades: Technical, as 20° C, 2° C, etc. (meaning distillation range); medicinal; C.P.; spectrophoto- metric. Containers: Bottles; drums; barreb; tank cars. Hazard: Toxic by ingestion and inhalation.Tolerance, 5 ppm in air. Flammable, dangerous fire risk. Explosive limits in air 1.8 to 12.4%. Uses: Synthesis of vitamins and drugs; solvent; water- proofing; rubber chemicals; denaturam for alcohol and antifreeze mixtures; dyeing assistant in textiles; fungicides. Shipping regulations: (Rail. Air) Flammable Liquid label. 2-pyridine aldoxime methiodide (PA t\,'f) C5~ H4CHNOH · ICH3• Antidote forcholinesterase- inhibiting pesticides of the parathion type because of its property of reactivating the cholinesterase hy removal of phosphoryl groups. pyridine-3-earboxylic acid. See niacin. 3-pyridine diazonium 0uoborate. Intermediate in manufacture of J-f1uoropyridine. Explodes when dry. 2,5-pyridinedicarboxylic acid. See isocinchomeronic acid. pyridine-N-oxide Cj H5NO. F.p. 67 .0° C. Soluble in water. Used as an intermediate. Hazard: Probably toxic and nammab\e. pyridine polymer. A polymer or copolymer of methyl- viny!pyridine and vinylpyridine; used for corrosion inhibitors and as intermediates for coatings and printing inks. 2-pyridincthiol-l-oxidc. See 1-hyd roxy-2-pyridine thione. pJ·ridinium brornid< Br2. Properties: Red p: (dee) with prelimi the dry state and ethanol and rela1 45% to 50% avail Use: Brominating bonds; mono-a including alipha1 carbony\s. Micro pJridoxal hyroehlor derivative of pyri Properties: Rhorr soluble in water a1 Use: Nutrition. pyridoxal phosphat1 5-pyridylmethylp CH,C,HN(OH)(' of amino acid inc group of various enzymes. It is clc Low toxicity. Derivation: Synth adenosine trip hos on pyridoxal, an, doxamine folio\~'( Uses: Nutrition; bi pyridoxine (vitam 3-H ydroxy-4,5-. group name des pyridine derivati Essential for the of amino acids a tryptophan; appc Pyridoxine is req of animals. Noflt, Sources: (Food): \ legumes, yeast, rr mercial): syntheti doxamine are p: reactions from is( Units: Amounts ar Uses: Medicine; n· hydrochloride). a I pha-pyrid yla mine beta-p yrid ylumine. 3-pyridylcarbinol C,H~NCH:OH. Properties: Caloric density (20:> C) 1.1 1.5455. Soluble ir Hygroscopic. Lo, Use: Intermediate. pyrimidine. One ( found in living n lowing comp!c:1e .\.\·.' t.._1., ., Early Photograph FCX Site . '•'\ I ,J •,,'I, ._. .. , .. : '. ' ' . ' --• Robert L Gordon. Director Food and Drug Protection DMslon na-i:nco,o1,rcD2p:,trr0"( d Ag<:ultl.>'e James A Graham • Commissioner WIiiiam G. Parham, Jr. • Deputy Commissioner FDC No. __ __,::w,J..L. ________ _ Raleigh. N.C. March 3. 1986 An OFFICIAL SAMPLE. represented or sold as ____:w:::e:=l:=lc....::w::.a.::.t::.er"---------• obtained by __ ..1.T~.1eE.......;Cc..aa.cc..rc..1u· kuec:.ir~,_....T.,_r ___ , an officer of this Department. on F"bnrnry 21, J 986 Labeled: 4 quart jars of w·ater from ~ell -;,:ell 500 ft. deep -pump in approx. 150 ft. down. Pump house & well approx. 750 ft. from FCX ·co. line. Mfr. or Dist. _C:::a::.r::..:n:.::a::.:t:..:i:.::';;:.fl:....:.:M:::i.:::l:.:.k_C:;::o"-'-. ,1.....:Pc..:O:......:B"'o"'x'--"S-=3-=3-=6.,_1 -'S"'"t""a"'t"'e,.,s'-'v"'i""l"'l~e~, -'-'NC"--2""8"-'6'-'7'--'7 ________ _ Retail Dealer.---------------------------------- RESULTS OF ANALYSIS: Pesticide Residues Analvsis: Measurable amounts of identifiable pesticide residues were not detected. CONCLUSIONS: No regulatory action indicated TO: Carnation Milk Co·: T. E. Carriker, Jr. Director BY: E. B. Williams, Food & Drug Administrator .. I I -• ,J~ Robert L GO<don. Director Food and Drug Protection DMslon / notr, Coroliro Depc,tfTY21"'( d A<;,<:ultlle James A G<0ham • Commissioner WIiiiam G. Pamarn. Jr. • Deputy Commissioner FDC No. --...u..='----------- An OFFICIAL SAMPLE, represented or sold as Raleigh. N.C. March 3, 1986 evaporated milk . obtained by __ _,_T.,_ • .:..· E=-. -'C"'a"'r'--'r'--'i'-'k'-'e""r...__-=J.,_r.,_. --· an officer of this Department. on --=F-=e-=b.:..r-=u-=a=-rv-'--'2"'1=-z..-'l'-'9:...:8:..:6:.,_ __ _ Labeled: FDC 8368 A-C Carnation Evaporated Milk 12 oz. can Code qHS 192· Mfr. or o isl. _...,Ce,a,.,r'-'-n"'a""t"'i"'o-'"n_C,e.o,:.:..'. .._.P_,O'---"B"'o~x_;.53"-3"-6~...,S'-'t'-'a'-'t'-'e"'s'-'v-"i-=l-=l-= e . , _ N " ' C " - - ' 2 ' - ' 8 ' - - ' 6 ' - ' 7 - ' 7 _ · -------~-- Reta ii Dealer _H_ac...rc...r_i_· s_ .. _.,T_e_e_t_e_r_S_t_o_r_e--'''---N_._M_a_i_n_S_t_. ,_, _M_o_o_r_e_s_v_i_l_l_ec.., _N_C_2_8_1_1_5 _______ _ RESULTS OF ANALYSIS: Pesticide Residue Analysis: Measurable amounts ·of identifiable pesticide residues were not detected. CONCLUSIONS: No regulatory action indicated TO: Carnation Co. · T. E. Carriker,. Jr. Director BY: E. B. Williams, Food & Drug Administrator • / nothCo,61,ro [)Qpc,ctmze(d Ag,:ultve FDC No. __ _,,8=6.,_9 ________ _ An OFFICIAL SAMPLE, represented or sold as -Robert L Gordon. Director Food and Drug Protection DMslon Jomes A Graham • Commissioner Wllllom G. Parham. Jr. o Deputy Commissioner Raleigh. N.C. March 3 1986 _ __,e'--v'-'a'-'p'-'o'-'r-=a'-'t""e"'"d~m"'i"'lk'-'--------, obtained by T. E. Carriker, Jr. . an officer of this Department. on February 21, 1986 Labeled: FDC 8369 A-C Carnation Evaporated Milk 12 oz. can Code qHS 282 Mfr. or Dist. Carnation Co •• PO Box 5336. Statesville, NC 28677 i: Retail Dealer Harris Teeter Store, N. Main St., Mooresville, NC 28115 RESULTS OF ANALYSIS: Pesticide Residues Analysis: Measurable amounts of identifiable pesticide residues were not detected. CONCLUSIONS: No regulatory action indicated TO: Carnation Co. T. E. Carriker, Jr .. Director BY: E. B. Williams, Food & Drug Administrator . . . •• Robert L Gordon. Director Food and Drug Protection DMslon James A Graham • Commissioner WIiiiam G. Parham Jr. • Deputy Commissioner FDC No. __::8:..:::6~0.::.2 _________ _ Raleigh, N.C. March 3, 1986 An OFFICIAL SAMPLE. represented or sold as _....;.EucY.ca-,,p,.o,._rc,.a.1..C e,c.du.....M.._1 ... · ]..,k,__ _____ , obtained by --"R""o;.,n;.,n"'-ie"-U"'n"'d~e""r'-'1,'-'·o~o""d'----· en officer of this Department. on _ _,_F.secsbccr_,,u.s,_a;,.rJ...y_2=-'5,_,__. _,1"9"'8"'6'----- Labeled: (unlabeled) Carnation Evaporated Milk 12 Fl. oz. QB6 214 Mfr. or Dist. _..iC.;aur::roli:aU:t:.ii.ll□.on_!..Coa_._. · ~· ...1P:10L.J:Bii:ot.:ix~5...i3...i3ll6~, ~S::i.twaaJC:.;e!!ss.ivoi.1l..1l..1eec.., _ll.NLC-"28"'6"-ZLZ'------------- -; Retail Dealer -----=------------------------------ RESULTS OF ANALYSIS: Pesticide Residue Analysis: Measurable amounts of identifiable pesticide residues were not detected. CONCLUSIONS: No regulatory action indicated TO: Carnation Co. Ronnie Underwood Director BY; E. B. Williams, Food & Drug Administrator ,. • • TERRY SANFORD .J. ALLEN ADAMS WILLIAM H. McCULLOUGH .JOHN 0. BEARD SANFORD, ADAMS, McCULLOUGH & BEARD ATTORNEYS AT LAW E. D. GASKINS,.JR. ROBERT W. SPEARMAN HUGH STEVENS CHARLES C. MEEKER CATHARINE BIGGS ARROWOOD BARBARA MILLS LARKIN WILLIAM G. PAPPAS ALFRED P. CARLTON.JR. CYNTHIA LEIGH WITTMER LISA M. NIEMAN STEVEN .J. LEVITAS BLAIR LEVIN .JOHN.J. BUTLER POPE McCORKLE m OF COUNSEL HEMAN R. CLARK HAND DELIVERY Mr. Harry Holladay P. 0. BOX 389 414 FAYETTEVILLE STREET MALL RALEIGH, NORTH CAROLINA 27602-0389 (919) 828-0564 CABLE ADDRESS SAMLAW March 3, 1986 Solid & Hazardous Waste Branch Environmental Health Section 306 N. Wilmington Street Post Office Box 2091 Raleigh, North Carolina 27601 RE: FCX Distribution Center at Statesville, North Carolina Dear Mr. Holladay, WASHINGTON, O.C. OFFICE 2000 M STREET, N. W. WASHINGTON, D.C. 20036 (202) 223-0200 NEAL A, .JACKSON MARTIN E. FIRESTONE DAVID P. TOWEY .JOSE:PH.J, LEVIN,.JR, FORD ROWAN .JOAN E, LANIGAN WILLIAM LIETH CARY OFFICE 8000 REGENCY PARKWAY SUITE: 350 CARY, NORTH CAROLINA 27511 (919)469-1089 CHARLES H. MONTGOMERY RENEEJ. MONTGOMERY NANCY H. HEMPHILL DAVID W. DANIEL We transmit to you a copy of the Environmental Evaluation Report received this morning from Fred C. Hart Associates, Inc. We understand that Dr. Page Fisher has discussed the topic of this report with you before. Due to the preliminary findings contained in the report, on behalf of FCX, Inc. , we have requested that Arch Purcell and Page Fisher draw up a proposal for further testing and evaluation of the site. We anticipate that this proposal can be made next week. Upon receipt of this proposal, we will talk with you further prior to implementing said testing. Also, by this letter we confirm our request that your Branch send us the appropriate forms so that we may supplement Page Fisher and our oral reports. \.__ /0 3 No7,,:-,rAif\ltv Fol<M TO 8£f.f:AJ/ Please let us know if you have any questions about the enclosure or any other matter related to this item. We will be back in touch with you shortly. WHM:CCM/sep Enclosure With best wishes, ,.,. ··---, ...... -....... cc: .. C. Page . Fisher ( w / out encl.) Charles A. Purcell (w /encl.) Stewart Hodges (w /out encl.) \' i I I I ! \. .f' ,, ' ·, ,. ,,- .i 't ,. ' " ,- . ' '' • I • '• ' ' I t '\ ,; 1_'_. I • ' . -·. --' -_12 Cl' ffl .l ·r--~~!.'_;J.: "'ii" Ii ,ii,, .. •J"~~J-tH;,-l ,J~::•.IJ•1• , . .,,,,,3.,,,, •~',ill ~ ·,~r11: ',,)! ~~ . ' t ' ' ·j ' ( 0 ;~ '...._. ' t?-v <f---.. I;; 'J ---z r-i -~ ' '0 b \r ~i '--.. S'-.. -~---: ! ·' ~-I ~-'-.; I I i I ,' !...,__ i 'f\ "'j--..1 ~ I~ --------! r ' " I ~ ' ~1 i I I ! ! I p t:1 I I I I ! I I I, : ! " '. j I I ! I ::"1 ~I ~ ~-~ 'I',., -'-i -"':- "-., ~ ~ 7'\ ~ ~ ~ l ~ ('l " ' \~ u-1 '-"" ~ '\) C> ..__ :--,-..C--,... ~ ;-... t, : = -. ' -\ ii() c::, Q '\:) "-t, ·"' ...,, ...c:, t , . "' 'I" 'ri ---Q. \v'\ ·• Ci' ' -~ : ~ (, ' ·N \ (" ()(o :C) !G' ' I ::"\ ! "'\ .Y\ ~ ~ I 'c:-' ,. \ ::i I '<:,. ' :~ i--0 I I ' ' I . ' -:~ , __ \\ ,.._ : "" i oQ I~ ,, \;.., i,f> cr-- ! I" I ~ I :~ },N ."-' ~ ~ \ -. ' : '-"l i;~ i :~ ~ '"" if'. ,c--_ j6' :, 1'· I• 'I'--_ 'I.,; ,<:r-. \~ ! io r ! ! ~ 1---, :-;:F::. !~ ' _.,.. ! I ! ', il i~ \'\ !o "<;) .,. i () "' :~ . ' : rJ ' ;C', ! : ' ~ I i'----. I--.__ ~ L~ ,--.__ i, I \t /f"\J !N "'I I~ ,N .1 i I ' ' ' ' :-----' l \"' ~ ~ :~ V : \ ,", ,\J\ .:I' \~ i' :, !N . "' "' 1--:01 ·"if.. ' v ' ;-L_ " ¼\ ,-;., '-<,j " '-.r\ "\.,'; . ' ~ I : I ': i ~! I, \i\' I '· ' i ' I ~ I ' ' i ' I I I : ~ I ' D ~ ' ~ ' I I h ii\ ,. ! I '-~ ii-! -· I i ~. I) ' ,-~ I i I ' l ' I i I i I i I I !lr, I 1~\ I I I ! 1 1 ' i ' ~-i ; ' ' i _, I q I • i I -, ' ' ' ' i I i ! ' "· I ' }:--\_, i ' -\ I ' ~~ i ! ' \' : I i ""' ~ ' I :~ I ! :"~ I \1. ' ' ' i I . . ' .. i,. ;, . . .... . ·- ti ENVIR0t-NENTAL EVALUATION RE POOT: F.CX Distribution Center 1620 West Front Street Statesville, North Carolina 28677 Prepared for: Southern States Cooperative, Inc. 6606 West Broad Street Richmond, Virgin i~ 232 30 Prepared by: Fred C. Hart Associates, Inc. 1110 Vermont Avenue, N.W. Suite 410 · Washington, D. C. 20005 February 27, 1986 .,,,.~·- / \ ! .... 1- . -,::.-,.. --· •· • D ISCLA !MER This report has been prepared for the exclusive use of Southern States Cooperative, Inc. The pL,pose of this report is to inform Southern States of the potential environmental 1 iobil ities associated with the FCX Distribution Center in Statesville, North Carolina. This report was completed in less than two weeks with limited analytical and geotechnical data. Additional data or facts 1113y alter the conclusions reached in this report. Therefore, Fred C. Hart ,/1.ssociates, Inc. wiil not accept 1 iability for any loss, injury or dama9= arising directly or indirectly from any use of, or reliance on this report by Southern States Cooperative, Inc. or any other party. ' • • TABLE OF O)NTENTS Paoe 1.0 Introduction .. • • . • .. • .. .. ... • .. .. .. .. .. . • .. .. • .. .. .. •• • . • .. • • l 2.0 Site Information ............................................. 3.0 Surrounding Land Use • • .. • • • .. • • .. • • • .. .. • .. .. .. • • • • . • • • • • • • • • 2 4.0 Monitoring Well Installation and Site Geology ................ 2 5.0 Samp1 ing and Analytical Results .. • .. .. .. .. .. • .. .. .. .. • • .. • .. • 5 5.1 Soil Contaminants .. • .. .. • .. • .. .. .. .. ..... .. • .. ••••••••••• 6 5. 2 Groundwater Contaminants ...................... •.••....... 6 5.3 Conclusions ................. ,........................... 7 6. 0 Pot en ti a 1 L i ab i 1 i t i es .. • • • • • • • • • • • • .. • .. • .. • .. • • • • .. • • • • • • • • • 7 6.1 Third Party Liability Risks .. : .......................... 8 6. 2 Regulatory Enforcement Risks • . • . • • • .. . . . .. • • • • • • . •• • • • • • 9 6.3 Financial Liabi1 ities .. .... .. .. .. ..... • • • • .. •• .......... 10 ATTACrf>1ENTS • -1- 1.0 Introduction Fred C. Hart Associates, Inc. (HART) was retained by Southern States Cooperative, Inc. to perform a prepurchase environmental evaluation of the FCX Distribution Center property in Statesville, lbrth Carolina. The need for an environmental evaluation was prompted by FCX disclosure to Southern States that up to ten (10) tons of_ DDT and DDD had been buried under the FCX warehouse prior to construction in 1969. In order to identify and limit any potential environmental liabilities associated with the proposed property purchase, HAAT implemented a rapid turnaround soil and groundwater sampling program at the FCX site on February 8-10, 1986. The results of the sampling and their significance are discussed in this report. It should be emphasized that this project was implemented and substantially completed within ten (10) days. This report should be viewed as a risk management tool for the exclusive use of Southern States Cooperative, Inc. Replicate and additional analyses as well as further hydrogeologic studies may alter the conclusions reached in this report. Therefore, HART w.ill not accept liability for any loss, injury or damage arising directly or indirectly from any use of, or reliance on th is report by Southern States Cooperative, Inc. or any other party. 2.0 Site Information The FCX site is currently a warehouse and distribution center for farm supplies, agricultural chemicals, and harct,,iare. kcording to the site manager, Mr. Lonnie Reed, former operations include pesticide dust blending and feed mill operations. The site began operations in the early 1940's. Pesticide blending was discontinued in 1969. The disposal of 5 to 10 tens of DDT and DD D took p 1 ace in July of 1969, while the current warehouse was under construction. A pit approximately 8 to 10 feet deep, 8 feet long, and 8 feet wide was excavated in the area that is now covered by the warehouse. The pesticide was taken out of its bags and dumped in the pit, which was covered with 6 feet of the on-site soil. hi 8-inch reinforced concrete slab, which is -2- the floor of the warehruse, was poured and covers the area of disposal. The area of disposal is approximately 50 to 60 feet from the front of the warehoose, and 50 to 60 feet from the nearest side wall, which adjoins an addition ..tiich was added in 1982. The majority of the FCX property is paved or covered with concrete. A narrow (4 to 6 foot) unpaved band surrounds the site on the north, west and sruthern sides. The eastern portion of the property has a small concrete pad on the northern side with the remaining area covered with gravel. Approxi_mately 25% or 1.2 acres of the property was not covered with an impermeable cover such as concrete, asphalt or structures. 3.0 Surrounding Land Use Land use in the inmediate area of the FCX site is both residential and industrial. State Highway southeast, passes just south Route 90, ..tiich runs of the site and rooghly gen er ally northwest to divides residential from industrial areas. South of Route 90 is residential, and r.orth of Route 90 is predominantly light industrial. Immediately to the west of the site is the Carnation evaporated milk plant. Imrrediately to the north, across the Southern Railroad tracks, is a Burlington Industries textile· manufacturing plant. Immediately to the east, across Phoenix Avenue, is an unoccupied lot currently used to store prefabricated utility sheds. Just north of this lot, to the northeast of the site, is a small school. To the north of the school are more residences. /lpproximately 1,000 feet northeast of the site is the Mil ls School. 4.0 Monitoring Well Installation and Site Geoloqy Four groundwater monitoring wells were installed at the site during the period of February 8-10, · 1986. Three of these wells were placed near the southeast corner of the FCX warehouse, and were completed as downgradient grounct,iater monitoring wells. building and was completed as One was placed at the northwest corner of the an upgradient monitoring well. MonitorinCJ well • -3- locations are presented on Figure 1. Grounct,,,ater was anticipated to be found under unconfined (water table) conditions, and the water table was expected to generally mimic the site topography, which slopes to the southeast. The three downgradient wells were placed at the southeast corner of the warehouse (downhill from the DDT/DOD disposal area) in order to intercept any contaminants migrating from that location. The upgradient well (MW-4) was pl aced near the northwest corner of the warehouse in . order to define background water quality, provide a data point for determining the water table configuration and hydraulic gradient. The downgradient boring which was sampled (MW-1) was advanced to a depth s ,..~.._.,,ei> of 45 feet. Competent bedrock was not encountered. Soil samples ~-e a red silty clay with sorre sand and mica to a depth of between 5 and 10 feet. From 10 to 45 feet, weathered bedrock, cir "saprolite," was encountered. The saprol ite was more deeply weathered near the surface, consisting chiefly of layers of silty clay alternating with layers of mica and other weathered minerals. Towards the bottom of the boring, the saprol ite was less weathered and more of the original structure was visible, but the material was still easily crurTbled by hand, and corrpetent rock was not encountered. The chief products of weathering of the parent gneiss are various clays. Small amounts . of residual mica and quartz were also present. Water was encountered during drilling between 30 and 35 feet bel0w grade. Soil samples were obtained from the upgradient boring (MW-4) and one downgradient boring (MW-1) using a split-spoon sampler at 5-foot intervals in order to define the site geology. Test boring logs for f-fw-4 and MW-1 are presented as Attachment 1. The remaining borings were not sampled with the split-spoon due to the time constraints on the project. The upgradient boring which was sampled (MW-4} showed generally the same geology as the downgradient boring (MW-1). This boring was advanced to a depth of 55 feet. Red silty clay with mica was encountered to a depth of between 5 and 10 feet, and saprol ite was encountered from 10 to 55 feet. From approximately 40 to 55 feet, the saprolite was white in color, and probably ~ FIGURE 1: FCX SITIE-SODL AND GROUi-JOWATEIAl SAMPLING LOCATIO~S . ' . \ 18uri."'7/.J :;cJJ. • 100& --· -.. -----·-----,.~..J ···-~-i± "'::·.::.:'"""'--=·t ·--·-·:1--·. I ) . • • ·---• - • -----1---,..,.,.._ . --f • • A. •• . \,, . .......... ,--. ~-'!-........ ... • \ • . . - -._. --_:_. -· ··-._. - - -.:. .. -• , _--+-'..,_.:;..,.··--r . ..11, -· • __ .. _ _ _ •• _ .• -·-. • • ...~_--:···_· .: • ~ .---11.U"-"!---=..;;...~-".\ .., . . ' ... ·,. . . ' --'"1MW•4 (105.18) :t. ': -•, . • • • I • ~ . . . . ~ ~ ' 1 . FCX qltiTRl■UTI . CENTIUI , • : \ \ \ -~ 1001 '-a;' • • ,--.. :1 .~----L---~-----------••-r-·-, X :----. -. -... - . ~ r---\--· ...., ...... _.,. ' ... ..so-.,;_ I •,GJ'':'W-2 (93./;9) :"':-,, c I L 0 MW-1 (88.84) . : ; .. , .... ~ ·-, ..... \ I ; \ \ • -----------. .._ ·--.. --~. 1002 -LEGEND l'i-COMPOSITE SOIL SAMPLE LOCATIONS 0-MONITORING WELLS WITH SURVl!VED PVC CASING ELEVATIONS . ([LEVATIONS Ill FEET ,DATlJM IS THE FLOOR OF TH.E.MhElf' fiAREHOUSE, SET AT U,.5 FEET) ~---pproxll'llato •~-hu,1,.,e DBrnnd DOD -~ 1003 • • -5- consisted alrrost exclusively of Kaolinite (clay) and small arrounts of quartz and mica. Water was encountered at a depth of approximately 40 feet during drilling. Well install at ion and sampling procedures are out1 ined in Attachment 2. Groundwater elevations were measured after the wells were developed. The groundwater gradient was determined by surveying well elevations relative to floor of the new blue sheet metal FCX warehouse (elevation 95.5 feet), since a U.S. Geological Survey reference benchmark was not in the area. Depth to water and water table elevation (relative to site building elevation) for each wen is presented in Table 1. Based upon water table elevations at the time the wells were installed, the probable direction of groundwater flw under the site is to the sooth. · We 11 Numb er MW-1 MW-2 MW-3 MW-4 TABLE l Relative Water Table Elevations F ex, Property Statesville, North Carolina Depth of We 11 Bering (feet) 45.0 50.0 4 9. 5 54.0 u.. Depth to Water from Top of llas ing ·(feet)· 31.21 35.80 (+.l) 35.95 - 41.00 (_:.5) Water Table 57 .63 57.79 5 7 .85 63.6 5.0 Sampl ina and Analytical Results Casing Top 88.84 93.59 93.80 105. 18 In addition to ground water sampling, five composite soil samples were collectec around the FCX site. The soil sample locations are indicated on Figure l and the sampling procedures are summarized in Attachrrent 3. Both groundwater and soil samples were analyzed for priority pollutant pesticides since they were the contaminants of concern. In addition, the groundwater samples were also analyzed for priority pollutant volatile organic fractions. • -6- These analyses were conducted to determine if other corrmon industrial contaminants were under the FCX site. Soil and groundwater samples were analyzed by York Laboratories in Monroe, Connecticut. The analytical results are presented in Attachment 4 and are surm1arized belc,,1. 5.1 Soil Contaminants Soil analyses indicated the presence of nine (9) pesticides or pesticide isomers. The highest concentrations detected were for chlordane, 8,000 ug/kg or parts per bill ion (ppb) at location 1002 and 4,4' DOT, .2,600 ppb·. at location 1005. Since the soil samples were composites of seven discrete samples, the maximum theoretical concentrations could have been as high as 56,000 ppb for chlordane and 18,200 ppb for DDT. Other pesticides detected at concentrations greater than 100 ppb were 4,4' OOE, Dieldrin, 4,4' 00D, and Methoxychlor. Alpha and Beta BHC (isomers of Lindane) and Endrin were detected at concentrations under 50 ppb. 5.2 Groundwater Contaminants Groundwater analyses indicated the presence of five (5) pesticide isorrers or metabolites and the presence of low levels of ten volatile organic cof1)ounds. The pesticide of gre.atest concern was the ga1T111a isomer of BHC 1-,+iich is the primary ingredient in the pesticide Lindane. Gamma BHC was found in three of the four wells tested, with concentrations ranging from 0.11 ug/1 or pob in the upgradient well MW-4 to 58 ppb in the downgradient wel 1 MW-3. The drinking water standard for' Garm,a BHC under the Safe Drinking Water Act is 4.0 ppb. In addition, the Alpha, Beta and Delta isomers of BHC were also detected along with a possible pesticide metabolite of Endrin Ketone. -7- The groundwater analyses also indicated the presence of twelve (12) volatile organic compounds, however, six compounds were either found in the sample blank or were detected bel°"' minimum detection limits but greater than zero. Trichlorofluoromethane was detected at concentration of 45 ppb in MW-4, tetrachloroethylene was detected at a concentration of 41 ppb in r,f,,/-2 and four other compounds were detected at concentration betwen 12 and 15 ppb. Overal 1, the monitoring well most contaminated with pesticide was ~-3. The well most contaminated with volatile organics was MW-2. 5.3 Coocl us ions Based upon the available monitoring data, the soils on the FCX site ··and the groundwater below it are contaminated primarily with pesticides, some of 11'1i_ch are at high levels. The DOT and 00D which have contaminated site soils and are buried under the FCX warehouse have apparently not migrated to g,o~ndwater under the site. These findings are not unexpected given the l CM solubility of these pesticides and the fact that the buried materials are .essentially "capped" by the warehoose. Furtherrrore, while most of the pesticides detected in soil samples are relatively insoluble, the Gamma isomer of BHC or Lindane is one of the most soluble pesticides detected in samples collected from the site. For example, Lindane is approximately 5,000 tin-es more soluble than OOT and 2,000 times more soluble than Chlordane. HART is unaware if Lindane had been handled and/or spilled at the FCX site. However, preliminary indications are that the Gamma BHC isomers is one of the most environmentally mobile pesticides detected at the site. 5.0 Potential Liabilities The potential environmental liability risks which, based upon avail able information, may be ass_ociated with the FCX site can be separated into third :iarty liability risks and potential Superfund or regilatory enforcement risks. This analysis considers both risks. • -8- 6.1 Third Party Liability Risks The third party 1 iabil ity risks presented by the FCX sites are related to the contaminated soil on the site and the groundwater under it. The risks presented by soil contamination relate to human injury via direct contact or inhalation of windborne dust. Most of the pesticides detected in the soils are persistant, chrCJ1ically toxic and are suspected human carcinogens. Available information indicates that Chlordane levels may be particularly high in comparison to national levels. For examole, the arithr:-etic average Chlordane concentration of the five soil samples collected at the FCX site was 1.88 mg/kg or parts per million {ppm). When the FCX avera~ concentration was Cl)'npared to average nationwide concentrations determined by the U.S. EPA between 1969 and 1980, the FCX site concentration was only exceeded on three occasions (see Attachment 5). Without further soil or arrbient air monitoring, the corrbination of relatively high levels of soil contaminants, a residential population south of the site and a school less than 1000 feet to the north presents a potential for third party 1 iabil ities. The third party liability risks presented by groundwater contamination is dependent upon demonstrating that the FCX site is the source of the cootaminants, particularly Lindane or Gamma BHC, and that human consumption of ground.later has, is or will occur. Ground.later concentrations of Lindane in one well under the FCX site is currently fourteen (14) times greater than allowable by Federal health standards for drinking water. Any downgradient consumer of groundwater with the L indane concentrations detected would be at risk of suffering adverse heal th effects. 't s, ~e. The Carnation Milk company is known to have a well adjacent to the FCX The use of the water from the Carnation wel 1 is currently unknol>Tl. The location of other ground.later users in the area is also unknown, however, the North Carolina Department of Natural Resources estimated that there are af+)roximately less than 100 wells currently in use in the Statesville area. • -9- .( Personal conmunication with Jesse Wells, N. C. Dt'R.) Until sufficient information indicates that no wells have, or are being used for potable purposes downgradient from the FCX site, a potential for third party liablity associated with groundwater contamination exists. 5.2 Regulatory Enforcerrent Risks The burial of OOT and 00D under the FCX warehouse building in 1969 required that a 103(c) notification be filed with Region 3 of the U.S. EPA pursuant to the Federal Uability Act (CERCLA). be filed by the seller even ts which may foll ow agencies are as foll Olis: Comprehensive Environrrental Response Compensation and It is HAAT's understanding that a 103(c) notice would prior to purchase of the FCX site. the sequE11ce of the receipt of the l03(c) notice by Federal or state 0 0 0 0 0 0 Serious attention by a re!JJlatory agency due to the late filing date, waste type and quantity involved; Inspection of the FCX site by re!JJlatory officials; Scoring the site using the Hazard Ranking System (HRS); Nominating the site for inclusion on the National Priorities List (NPL) if the HRS score is over 28.5; Requiring monitoring, clean-up or rerrediation under CERCLA or state environmental statutes; and/or Assessrrent of financial and/or criminal penal ties. HA<T scored the FCX site using the HRS to estimate how regulatory agencies might view the site. Using available information, the FCX received an HRS score of 22.4 (see Attachment 5). While this score would not qualify for inclusion on the NPL, it is a score which would most likely receive • -10- serious attention by the regulatory agencies. Regulatory actions would likely require a minirrum of soil and ground,,/ater sampling and analysis to a maxirrum effort including groundwater clean-up. 6. 3 F in an c i al Li ab i l i ti es Financial liabilities. associated ~,ith the FCX site could include third party lawsuits claiming adverse health effects, adverse publicity, protracted litigation and e~vironrrental monitoring and clean-up costs. Most of the potential liability costs associated with the FCX site are non-quantifiable, hO'.-iever, environmental monitoring and clean-up costs can be estimated. Based upon HMT's experience, monitoring and possibly clean-up of the FCX Statesville site may be required by regulatory agencies. Assuming that a full clean-up is required, the potential cost to the site owner, exclusive of legal and actninistrative costs could range from $875,000 to $1,305,000, in 1986 dollars. These costs are summarized in Table 2 below. TABLE 2 ESTIMATED CLEAN-UP COSTS F CX Property Statesville, North Carolina Item l. Soil sampling and analysis 2. Remove and dispose of contaminated soil. (Assumes 100' x 100' x3' or 1100 cubic yards @ $300 per cubic yard.) 3. Repair and regrade site 4. Ground..later clean-up and recovery sys- tem. (Assurres operation for 3 years with discharge of treated ground..later to public se,ier) a. Well construction (10-12 wells) b. Operation maintenance and analysis (for 3 years) 5. T0T~.L ESTIMATED COST RANG: CO'S t Range $ 50,000 -$ 70,000 330,000 -330,000 20,000 -30,000 l 00 , 000 -200 , 000 $375,000 -$ 675,000 $875,000 $1,305,000 ~ [LEV. DtPTH S-lMPU ~ lF"EE'T) (F"EIT1 TYPE [ DtSCRIPTl0H --•------ -------- --..... ----- --.... -' ---- ------..... - --..... ----- - - ----..... ---.... -- - -- ------,_ - --..... ---..... - rr , w,-r., clc.; ;-i. t:-1 ('.:, <.--r-I .1. _...,i~ ,._. I /C' ~{,ilif Ci :5 c,Jov€? !':: 5 • .;.::,'' ~:,/' i'O f; f~) SC' ,, ; t C< :0 Ci/; C: Vt/ iT ye 1::r.-., -l,01.,.,;,·, rclcr 1.:ii. c: -3o.c Sar,c l.1t Grr.,..1 .;,l ... lt lcoi-::,/ rT (Y, ; c °' -r, , h rr < I -_, ,;, - - • ,,. I it" V ,'-I '- 5:, , • "\'.: c;. ~ C: l, ovt? IT TO ~I./~ l"A:EO C. MART ABBQCIATIHl, INC. , F1£Lo ENGINEER, z. e. w. :-r, ri n.kCTRAHON <> PIESISTAHCE ~ (BL~ Kl! FOOT l =· 10 SO SO WAT£.R C0I/TENi (PERCEXT) 20 -0 I I I cl,/>/) WASHINGTON, D.C. • • ATTACf-MENT 2 WELL INSTALLATION, DEVELOPMENT AND SA'>1PLING ffiOCEDlPES l ..... I t_ 1 ES 1 .... - ,--,_ --- ,---·-r---- .... - r-- r-- ,-- ,-------- .. ~~--.. --.... --- I-- ,----- - -- -------- .... ------- r -.... - I---- ,_ -,-· ----- 80R' '(, LOC, I ss DESCRIPTION llj n.NCTRAHON .., RESl9TAHC[ ri (8LC7-b'S POI FOOT) ::, 10 SO !!O 'f -e, -IC WATUI C:ONTENT (PtRC4HT) 20 40 ' 5 c =e-c::; ~ " .t:,..,6 d "'· ~-""P +1.,.J;.. ________________ . --..., ___ -~,.: .. ~ ;....,1-'b-t---+---+.- i 6. 5'-.::i ~ 0 5 '-' ;_ C· ,; ! r [T rr T rr Ob t:...,,, ~ w ,· h rr!,··,,-'le--,y ~ 1,.J/,,i't-~ lc-;,1cts. '33.5-,35.0 S« f,..c I ih so.,,,c:<-o.::, c, bev<;o lf3. ) -1../ 5. 0 s~ ,-, (-C-. s c,(;;cve 1.D Y6.S 3. - I FFIEC C. HAFIT ASBCCIATl!B, INO::. , WASHINGTON.· D.C. ., • Well Install at ion, Develop:nent and Sampl ina 1/el 1 Jnstal lation The four rronitoring wells were installed during the period of February 8 through 10, 1986. The drillinq contractor was Subsurface lnvesti9ations, Inc., of Charlotte, North Carolina. The wells were drilled in the order in wtiich they are nurrbered using a Q,IE 45 hollow-stem auger rig. Soil samples were obtained from borings MW-1 and M',./-4 using a split-spoon sampler at 5-foot intervals in order to define the site geology. [\Je to tirre constraints, borings MW-2 and MW-3 were not sampled at 5-foot intervals, although samples were obtained from selected intervals. The borings were advanced to a depth of between 10 and 15 feet below the depth where water was encountered dur.inq drilling. The augers were withdrawn, and the casing was installed in the open boreholes. The casing and screen used· were made of 2-inch diarreter schedule 40 PVC joined with friction coupl inos (no solvent). The screen had machine-slotted 0.010 inch perforations and a bottom plug. A small amount of duct tape was used to hold the friction couplings together during instal 1 at ion. Due to time constraints, the preferred threaded-joint casing and screen could not be obtained. The wells were packed with washed mason's sand to at least two feet above the screen. Bentonite pellets were installed above the sand for at least a two-foot interval. The remainder of the boreholes were grouted to the surface using cerrent. A 4-inch square steel protective casing with locking cap was cemented into place at the surface, .and a cerrent collar was built up around the casing to prevent infiltration of surface water into the borehole. The auger flights and drilling tools were washed between boreholes using tap water from a garden hose. All soil was removed. '../ell DevelopTient and Sampling All wells contained approximately a 15-foot water colurm. All wells could be bailed down by removing approximately ten one-1 iter bails. Wells then required two to several hours to recover. Wells MW-1, MW-2, and M.1-3 were bailed down at least four times prior to s-ampl ing. Bailing rerroved most of • -2- the sediment from the wells, al though a small amount of sediment remained. Alternative rrethods of development would probably have involved adding water to the wells, due to the s lo,,, recovery. These were not used due to the requirement that an undiluted sample be obtained. Problems were encountered during the installation of M'..1-4 (upgradient). During sand pack installation, the top 2D-foot section of cas·inci become uncoupled from the lo,,,er section of casing. Approximately five feet of sand entered the casing before the error was discovered and corrected. The casinq was re-coupled in the borehole with no apparent problem, and the well installation was completed. Most of the sand in the casing was removed by bailing. At least 50 one-liter bails of water and sand were removed from MW-4-prior to sampling. MW-4 was not allowed to completely recover, but was bailed more or less continually, in order to remove sand from the bottom of the well. The sand from the well appeared clean--there were apparently no other materials (soil, bentonite, grout) in the casing. The wells were purged and sampled using pre-cleaned stainless steel bailers lowered on new, 1/8-inch nylon cord. The bailers had previously been cleaned using Alconox detergent follo,,,ed by a tap water rinse, then a distilled water rinse, then a pesticide-grade methanol rinse, air drying, and · another distilled water rinse. The bailers were then tightly wrapped in aluminum foil, and transported to the site. As each bailer was unwrapped, it was rinsed with distilled water prior to insertion into each well. Because only three bailers were available; one had to be de-contaminated and re-used to bail and sample the last well, MW-4.'u,o'ff'~e bailer was washed using detergent, followed by a tap water rinse and a distilled water rinse. The samples were taken on t-'onday, February 10, 1986. Samples were collected in bottles provided by the laboratory via an air freight shipment. Sample labels and chain-of-custody forms were completed, and the samples were shipped on the evening of February 10 via overnight air freight. The laboratory contractor was York Laboratories, a division of York Wastewater Consultants, Monroe, Connecticut. Table 1 provides a summary of well construction data. • TABLE 1 SUMMARY OF GROUNDWATER OBSERVATION POINTS FCX WAREHOUSE STATESVILLE, NORTH CAROLINA SUBSURFACE INVESTIGATIONS, INC. PROJECT NUMBER 1594 MATERIAL SUMMARY: CAP CASING SCREEN LOCKING 4" SQUARE STRUCTURAL TUBE; CARBON STEEL 2 INCH DIAMETER SCHEDULE 40 PVC; FRICTION COUPLINGS, NO SOLVENT; SET IN GROUT ABOVE THE BENTONITE PELLET SEAL COMMERCIAL SCHEDULE 40 PV~ SCREEN SA~Q PACKED IN WASHED MASONS SAND. (0.0IOu .Slo'iJ FOR STANDARD PENETRATION RESISTANCE, SEE TEST BORING RECORD. POINT STICK UP CASING SCREEN SAND PACK BENTON I TE NUMBER ABOVE FROM TO FROM TO FROM TO PELLET SEAL FROM TO WELL 1 *2' 0' 35' 35' 45' 33' 45' 31' 33' WELL 2 *2' 0 ' 40' 40' 50' 30' 50' 20' 30' WELL 3 *2' 0 ' 39.5' 39.5' 49.5' 37.5' 4 9. 5' 19.5' 37.5' WELL 4 *2' 0 I 44' 44' 54' 42' 54' 30' 42' *THese numbers are approximate'. • • Soil Sampl ino The objective of the soil sampling program was to collect representative composite samples, which when analyzed would document any surficial contamination at the facility. Each soil sample was collected with a separate pre-cleaned trc:Mel for each sample region. Tro.-iels were cleaned with tap water, a phosphate detergent wash and then rinsed with distilled water. The soil samples were placed in laboratory supplied pre-cleaned glass jars and shipped overnight for analysis. Five representati{e sample regions were chosen around the periphery of the facility and .a composite sample was obtained from each region (see attached map). The sample taken at each region contained a composite of soil taken from 4-7 locations within that region. Sample #1001. Taken along the fence on the west side of the facility. Composite of 4 sample locations. Sample 111002. Taken along the sidewalk and parking lot on the south side of the facility. Samples taken from grass area and sediment in parking lot. Composite of 7 sample locations. Samole #1003. Taken along the sidewalk at the extreme south-east portion of the facility. Composite of 5 sample locations. Sample #1004. Taken in the extreme south-east corner of the truck loading area. Composite of 6 samp.le locations. Sample #1005. Taken al oog the back of the building adjacent to t~e railroad tracks. Emphasis was placed on loading and transfer areas. Composite of 7 sample locations. () • ....c .., -1 .I "' • < ., ... .. . • -~j !t .. ' ! .... !i . t ~:-,: : ,! .... ' i I I I •• .J ..•. " ..... , .. . ! ' .. Q' ~ Jt • •• ' ,. ,~ ; ;, :~ .. J ~ ~ ' -+ ' • -:, 0 • . ' □· ~ ~, J ...;.. ' ~ ..., ., ~ I l I I \ I i \ \ \ ' ' ; '·c \ \ \ I ~ I' ' • i ' l \ l 2. l • i \ • I • ' I • ~ \ • :-, ' • i > ' ~ t • a • ¥ I ~ 3 • 1 • ' ! ;:: • • f ! • e i : • J ; • ,, ' . ' ' ' ,j "' ~ CI; February 14, 30860-639 FRED C. HART ASSOCIATES 1110 Vermont Avenue N.W. Washington, DC 20005 Attention: Mr. Mark Merrel PURPOSE AND RESULTS Five (5) soil and four (4) Laboratories for analysis. in the following Tables. Prepared water samples were submitted to York Preliminary results are tabulated Curran st JCC/md The liability of YWC, Inc. is limited to the actual dollar value of this project. ~ • ' \BLE 1. EPA PRIORITY POLLUTANTS 1...:..IENT FCHAZFCX PESTICIDESLPCB's JOB# 30860-639 All Results ReEorted as ug/Kg, ~ Sample Identification Dilution Factor ,........----.... " /u,,.;,.,,,·,,._G ) ! . ' / 10 5 5 \ , _________ ~ethod Blank I • D. 2{12[86 2[12[86 2/11[86 2[11[86 2[11[86 Soil Soil Soil Soil Soil Lower Limits of 1001 1002 1003 1004 1005 Detection with :::omEound 0639001 0639002 0639003 On39004 0639005 no Dilution alpha BHC u u u u 9 0.80 beta BHC u u u u 29 0,66 gamma BHC u u u u u 0,54 delta BHC u u u u u 0,80 Heptachlor u u u u u 0,66 Aldrin u u u u u 1.3 4,4' DDE 13 420 53 40 250· 1.3 Dieldrin 2,7 140 u u 460 1.3 4,4' DDD 20 630 31 55 290 1.3 Endrin Aldehyde u u u u u 1.3 4,4' DDT 26 150 96 100 2,600 15 Chlordane 240 8,000 413 760 u 40 Endosulfa·n I u u u u u 1.3 Endosulfan II u u u u u 1.3 Endosulfan Sulfate u u u u u 9,4 •Endrin u u u u 46 1.3 Heptachlor Epoxide u u u u u 1.3 Toxaphene u u u u u 220 u -See Appendix for definition. e • rABLE 1 EPA PRIORITY POLLUTANTS Aqueous LIENT FCHA/FCX PESTICIDKSLPCB's ?\\tl\\\\i~J1 ,OB If 30860-639 All Results Reported as ug/L. Sample Identification ~tt\:t,~,~ Dilution Factor 1 1 20 1 . ~ts .. -~-r.i _'i?.P t~ Lua) t1'-d1. Method Blank I.D. 2/12/86 2/12/86 202/80 2/12/86 Lower Limits of MW-1 MW-2 MW-3 MW-4 Detection with Compound 0n39006 0639007 0639008 0639009 no Dilution alpha BHC 0.87 0.09 34 0. 12 0.01 beta RHC u u 5.6 u 0.01 gamma BHC 0.33 u 58 0.11 0.01 delta BHC u u 13 u 0.01 Heptachlor u u u u 0.01 Aldrin u u u u 0.01 4,4' DDE u u u u 0.01 Dieldrin u u u u 0.01 4,4' DDD u u u u 0.05 Endrin Aldehyde u u u u 0.05 4,4' DDT u u u u 0.05 Chlordane u u u u 0 .1 0 Endosul.fan I u u u u 0.01 Endosulfan II u u u u 0.05 Endosulfan Sulfate u u u u 0.05 Endrin u u u u 0.05 Heptachlor Epoxide u u u u 0.01 Toxaphene u u u u 1.0 u -See Appendix for definition. • • TABLE 2 30860-639 FRED C. HART ASSOCIATES/FCX ADDITIONAL PESTICIDE Rr.SDLTS (non priority pollutant pesticides) 0639007 -Endrin Ketone 0,39 ug/L 0639008 -Endrin Ketone 3,0 ug/L 0639005 -Methoxychlor 670 ug/Kg ~\BLE l .I ENT JOB II 3 FCHA/FCX 30860-639 i llution Factor • EPA PRIORITY pOLLIJTANT VOLATILE COMPOUNDS • All Results Reported as uu1. Sample Identification 1.00 1.00 1.00 1.00 P'{f))flNfJl! Aqueous nci uiv;/flARY •-. RELEASE 1.00 v,! Method Blank I.D. >Al573 >A1573 >A1573 >Al573 >A1573 Lower Limits Method Blank MW-1 MW-2 MW-3 MW-4 Compound 0639006 0639007 0639008 0639009 nlorometha.ne uromomethane vinyl chloride hloroethane ethylene chloride trichlorofluoromethane ·:rolei.n c.rylonitrile 1,1-dichloroethene 1,1-dichloroetha.ne rans-1,2-dichloroethene ¥hloroform 1,2-dichloroethane ,1,1-trichloroethane a.rbon tetra.chloride bromodichlorornetha.ne --chloroethylvinyl ether ,2-dic~loropropa.ne tra.ns-1,3-dichloropropene trichloroethylene · enzene ~is-1,3-dichloropropene dibromochlorometha.ne ,1,2-trichloroetha.ne romoform tetra.chloroethylene ',1,2-2-tetra.chloroetha.ne .oluene chlorobenzene Rthyl benzene u u u u lJ u u u u u u 3J u u u u u u u u u u u u u u u u u u *U -See Appendix for definition. *J -See Appendix for definition. *B -See Appendix for definition. u U· u u lJB u u u 5J u u lJB u 3J u u u u u u u u u u u 9J u u u u u u u u 2JB u u u 15 12 15 lJB u 15 u u u u u 2J u u u u u 41 u u u u u u u u 2JB u u u u u u lJB u u u u u u u 3J u u u u u 2J u u u u u u u u 2JB 45 u u u u u 3JB u u 6J u u u u lJ lJ u u u u u u lJ u u of Detection with no Dilution 10 10 10 10 10 10 100 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 -A..BLE LIRN'l' JOB II 3 FCHA/FCX KPA PRIORITY POLLUTANT VOLATILE COMPOUNDS 30860-639 All Results Reported as ug/L, Sample Identification ilution Factor Method Blank I.D, Cor.,nou nd hl·oromethane _romomethane vinyl chloride hloroethane ethylene chloride trichlorofluoromethane -crolein crylonitrile 1,1-dichloroethene 1,1-dichloroethane rans-1,2-dichloroethene .... hloroform 1,2-dichloroethane ,1,1-trichloroethane · ~rbon tetrachloride bromod i_cr. loromethane n-chloroethylvinyl ether ;2-dichloropr6pane trans-1,3-dichloropropene trichloroethylene enzene _is-1,3-dichloropropene dibromochloromethane ,1,2-trichloroethane romoform tetrachloroethylene ',1,2-2-tetrachloroethane oluene chlorobenzene P.thyl benzene 1.00 >Al573 Trip Blank 1 0639010 u u u u 6JB u u u u u u 3JB u u u u u u u u u u u u u u u u u u $LJ_ -See Appendix for definition. *J -See Appendix for definition, *3 -See Appendix for definition. 1.00 >Al573 Trip Blank 2 0639011 u u u u 6JB u u u u u u 2JB u u u u u u u u u tJ u u u u u u u u Lower Limits of Detection with no Dilution 10 10 10 10 10 10 100 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 APPENDIX •U -Indicates that the compound was analyzed for but not detected. *J -Indicates that the compound was analyzed for and deter- mined to be present in the sample. The mass spectrum of the compound meets the identification. criteria of the method. The concentration listed is an estimated value, which is. less than the specified minimum lower limit but is greater than zero. *B -This flag is used when the analyte is found in the blanks as well as the sample, It indicates possible sample con- tamination· and warns the data user to use caution when applying the results of this analyte. *D -Sample extract was diluted by the factor listed due to the sample matrix and/or concentration levels. All method lower limits of detection for this sample are necessarily increased by this dilution factor. • ATTACI-MENT 5 CHLORODANE OONCENTRATIONS IN SURFACE SO !LS OF SELECTED U.S. lPBAN AREAS • OIDIICAL/EUW:-.'T cnlCENfP.ATIOOS IN SURFACE SOILS OF SELECTED U.S. URBAN AREAS, PPM (or rrq/kg) dry weight QlEl-lICAL: Technical Olloroane (CAS RN:_ 12789-03-6) . (St 058202) Location Bc)kersfield Camden Houston Manhattan Miami Milwaukee Salt Lake City Waterbury Auqusta O1arleston Olevenne Grand Rapids Greenville Honolulu Percent Calendar Total No. Positive Detected Values Arithmetic Yr. Sl'ITlOlecl of Analvses Detections Minimum M/\ximun Mean CA 1969 50 30.0 0.07 20.48 0.78 NJ .1969 50 16.0 0.39 5.90 0.36 TX 1969 50 34.0 0.04 12.94 0.66 -KS 1969 50 40.0 0.03 4.86 0.30 FL 1969 50 64.0 0.04 16.R7 1.59 WI 1969 50 34.0 0.05 10.21 0.45 lTT 1969 50 38.0 0.02 7 .50 0.41 CT 1969 50 28.0 0.02 8.74 0.96 ME 1970 27 11.l 0.21 0.27 0.03 SC 1970 27 25.9 1.01 1.35 0.12 WY 1970 19 5.3 8.99 -0.47 MI 1970 23 43.5 0.15 6.58 0.71 MS 1970 28 7.1 0.37 1,40 0.06 HA 1970 21 28.6 1.00 13.90 1.27 Source: U.S. Envirorrnental Protection Agency, Office of Pesticides and Toxic Substances, Urban Soil Monitoring Program. Est1mate<l ,.ecrnetric Mean -0.004 0.009. * 0.056 0.004 0.041 QIEMICAL/EU:MENT CDNCEN'ffil\TIONS IN SURFAG: 9:JILS OF SELECTED U.S. Ul-0:lAN /\R£AS, PPM (or. mJ/ky) dt·y weiyht CHEl-lICI\L: Technieal Chlordane (CAS RN: 12789-03-6) (S# 058202) Peccent Estimated calerdar. Total No. Positive Detected Values Arithmetic Gecmetric Location Yr • S/fl\D 1 eel of Analvses Detections Min1mun Max1mUTI Mean Mean Monullis 'IN 1970 28 1.4 0.11 8.02 0.36 0.014 Mobile AL 1970 29 24.l 0.10 2 .so 0.18 0.016 Ph ilade lph ia PA 1970 26 42.3 0.18 4.59 0.76 0.07~ f\Jrt.land OR 1970 25 12.0 0.40 0.59 0.06 0.006 Ridmond VA 1970 27 18.5 0.18 6.42 0.51 0.015 Sikeston MO 1970 27 7.4 0.30 1.19 0.06 0.004 Sioux Citv IA 1970 22 18.2 0.30 3.00 0.24 0.013 Wilmir,,iton DE 1970 27 7.4 0.04 0.07 <0.01 0.002 llill t iiror e MD 1971 156 36.8 0.01 12.35 0.21 0.016 Gadsden AL 1971 55 5.1 0.04 0.46 0.07 0.002 HartfOl'.d CT 1971 48 47.9 0.02 140.69 4.00 0.06 Macon GA 1971 43 25.6 0.07 0.91 0.08 0.012 Newoort News VA 1971 78 12.8 0.09 7.29 0.16 0.007 Des Moines IA 1972 90 20.0 0.04 85.0 1.70 0.012 2 Cl-lEMICAL/ELEMENT (X)NCENTHATIONS IN SURFACE SOILS OF SELOCIBD U.S. URBAN AREAS , PPM ( or ll'<J/kg ) d cy we iyh t CHElHCAL: Technical Chlordane (CAS RN: 12789--03-6) (S# 058202) Peccent EstunatoJ Caleruar Total No. POsitive Detected Values Ari ttrnet ic Gecmetric Location 'fr: , Samnl ed ·of Analyses Detections · Minimun Maxirnun Mean Mean / F1tchburq MA 1972 35 5.7 0.36 0.39 0.02 0.002 Lake Charles [A 1972 70 4.3 0,08 0.29 0.01 0.003 Pittsburah PA 1972 189 7.4 0.04 45.00 0.50 0.004 Readin:i PA 1972 50 6.0 0.59 1.19 0,05 0.003 Evansville IN 1973 82 23.2 0.04 77.02 1.29 0.018 Greenville SC 1973 86 9.3 0.02 2.23 0.06 0.004 Pittstield MA 1973 45 11.1 0.10 1.13 0.06 0.005 ' Ta=rna WA. 1973 95 14.7 0.02 16,69 0.30 0.009 Washi=ton oc 1973 132 33.3 0,02 80.55 1.01 0.020 San Francisco CA 1974 164 18.9 0,01 90.23 1.01 0.01., Pine Bluff AR 1974 59 13.6 0.03 0.97 0.05 0.006 Gary IN 1974 85 17.6 0,01 51.73 1.59 0.013 C:Urhan NC 1974 66 ND sorimfield IL 1974 72 36.1 0.01 47 .14 0.91 0.028 3 Olr.MICAL/ELEMENT CDNClsNTRI\TI~lS IN SURFACE SOILS 01:' SELECTED U.S. URlil\N ARE:J\S, PPM (or mJ/ky) dry weiyht CHDIIC'.AL: Technical Chlordane (CAS RN: 12789---03-6) (S# 058202) Percent lsstimatoo Calerrlar Total No. Positive Detected Values Ari t.trnet ic Geanetric Location Yr. Sanpled of Analyses Detections Minirnun Maxirnun Mean Mean Haker sf ield CA 1975 42 38.l. 0.01 11.16 0.34 0.012 Carden NJ 1975 50 30.0 0.01 6.67 0.38 0.014 llouston TX 1975 48 58.3 0.01 286.83 8.52 0.084. Manhattan KS 1975 50 42.0 0.02 8.69. 0.78 0.053 Miroti FL 1975 50 50.0 0.01 13.86 0.45 0.032 Milwaukee WI 1975 47 27.7 0.06 6.46 0.33 0.019 Salt Lake City ITT 1975 50 48.0 0.01 0.69 0.09 0.023. ' l'laterbury CT 1975 44 72.7 0.01 15.69 1.44 0.117 MJUSta ME 1976 25 ND Charleston SC 1976 26 65.4 0.02 3.14 0.28 0.03•:· Chevenne WY 1976 19 21.1 0.03 0.15 0~02 0.005 Grarrl Rapids MI 1976 22 27 .3 0.04 0.36 0.06 0.016 Greenville MS 1976 28 14.3 0.01 0.19 0.01 0.003 Horolulu HA 1976 21 66.7 0.04 108.57 8,25 0,307 4 OiEMICAL/F~LrnENT mNCENTHJ\TIONS IN SURFi\CE SOILS Of SELECTED U.S. URBAN AREAS, PPM (or rrg/kg) dry weight CHEMICAL: Technical Chlordane (CI\S RN: 12789-03-6) (S# 058202) Percent EstimatorJ Calcrdar Total No. Positive D-c,tected Values Ar it.hnetic Geanetric lncation 'fr • samn 1 eel of Analyses Detections Minimun MaXimun Mean Mean Manphis TN 1976 28 46.4 0.01 0.54 0.06 0 .016 · Mobile AL 1976 24 33.3 0.01 0.14 0.03 0.009 Philadelphia PA 1976 24 37.5 0.03 1.75 0.22 0.026 Fortlan::t OR 1976 25 28.0 0.02 1.38 0.10 0.009 Rict.11000 VA 1976 27 55.6 0.03 5.94 0.68 0.066 Sikeston 00 1976 27 25.9 0.02 13. 71 0.52 0.009 Sicux City IA 1976 22 27.3 0.04 1.46 0.13 0.014 Wilmirnton DE 1976 25 24.0 0.02 0.18 0.02 0.005 · Baltimore MD 1977 Not SclllDled Gadsden AL 1977 55 Hartford CT 1977 42 23.8 0.19 32.55 1.78 0.03 Ma=n GA 1977 41 14 .6 0.07 3.08 0.10 0.01 N-t News VA 1977 -78 14.1 0.02 . 26.0 0.42 0.01 Des Moines IA 1978 Not ,aannled 5 OIEMIC,\L/ELEM!:."NT <DNCENTRATIUNS IN SURFACE SOILS O~' SELECTED U.S. URBAN MEN:;, PPM (or tn;i/kg) dry weight CHDIICAL: Technical Chlordane (CAS RN: 12789-03-6) (S# 058202) Percent EstimatoJ Calendar Total No. Positive Detected Values Ar i t.hnc t ic GL-'Cllletl'. ic Location 'ft. S"""'led of Analyses Detections Mimmun Maxunun Mean Mean f'it.chburo MA 1978 36 5.6 0.23 0.39 0.02 0.002 Lake Charles [A 1978 70 ND 0.00...,.--Pittsburuh PA 1978 190 7.3 0.04 -35.66 0.54 I Headiru PA 1978 51 3.9 0.45 9.93 0.20 Evansville IN 1979 82 Greenville SC 1979 86 Pittsfield MA 1979 45 Tacona 1 ~ 1979 83 Washimton oc 1979 123 San Francisco CA 191:10 Sc111pled but •--not analyzed i'inG Bluff AR 19UO sanploo tJ.Jt not analyzed Gary IN 1980 ScS11pled Out -1 not analyzed .b _...... 01EMICAL/ELl:l'IBNT CDNCENTRATIOOS IN SURFACE OOILS OF SELOCI'ED U.S. URBAN AREAS, PPM for my/kg) dry weight CHF1'1ICAL: Technical Chlordane __ {CAS RN: 12789--03-6) (S# 058202) Percent Estimated Calerrlar Total No. Positive Detected Values Ari ttrnet ic Geanetr: ic Location Yr. Si'llloled of Analvses Detections M1nunun Maximun Mean Mean . Durhi'll\ NC 1980 Sat1ploo but not analvzoo Spr ingtield IL 1980 Sanpled but ._ not analvzed ND = Not Detectoo • 7 .......... • ATTACf-MENT 6 HAZAAD R/l.NKING SYSTEM {1-f<S) SCORE SHEET AND OOCLMENTATJON IIAZARD f!AN~l~ SYSTEM SCORE SHEET and DOCOOlilATJOH Fllltl C. k.Atl't A$.50CU..Tt.S.. "-t • Oro..o,o c-Jttr 111o,,,1o "°"' S-1 ~l'""G foclOI Aat,o"Ot YPVO ~ llcoto ts.■ .. , 4t,,,i .. 0,,0\ pllO< D,cc,o 111,e,t_, [!) OI, l E oo0 ci.i. ... • ® ' 45 es a., 0 et,.t.o. ~ ,_ b .,.._, e i:,cor,, GI C'ti.~1911M ('!) ri es , "flKI IIH4N 1\1 f;I-. e _,, Gf e. p, c 11 s ED t... ID [!) ~O,O~U:U a.a ~ ti> AQvttor of II , a , • 0 C.C-Offi ~ f'roelpiUlt!Ofl . • , I , . ' a Pe, F yt,ll'IJ Ii/A ... e I I a ' a ~!\lf111o0 Z- Pt, ,,..cal '"'" • 1 I a t a 'i'Olll AIM1' Chnc'ltt"O"a ;.oc,,,, Ill ll) ~ -I) t I I 1 I s..a rn ~~~1dcl S.4 Veou=l'ttlPersl-o a ri 0 UIS®) 1 18 Ill tllw,OCMWaa,a •©a I • 11 ti ' G 1 1 ll OuD,nlny • . ,_,, __, Ola, m:ur• u -1 s-e 19 Ill lil taraeu , G) a ~. ~ 1.5 . erllUftdW.terUN 0 • D1a"tao ,co ID N_..i l ,i • e ii'° a, Vlf ell I Popul&IIOn " " Se,1 uaO 14 20 12 C tOIAl1~115-9 26 a [!) Iii m,,o m II U. -'llply (D a rn a rn ·-1 bD,__,.,. m R l!l R (!}am '2230 57.DI rn cw.oe11ne m IIJ57..230 and lftl4lll!lyby ~ 'o••38. 77 . GROUND WATER ROUTE WORK SHEET 'I • a.,,tc:o Vl11ici ~ ~ Oloo1 Aul04d Vdve IIWI\► ti,,. Aol. ~·-~~) ,_ \l,c,o,9 a:-~1'oft) Cl) =~w;;c~ Iv a ' 0 Q G.1 Ci Wt$M ~ b ~ ll 0110 cl~ pc;.::,;,:! b ~ ~ C';l 1:,;c,e, ~ ~ b ~ o 'ld"3 c,I II, p::: ~ lD ~ @ ~C>a!!dcl\A:s 4.2 Pcd,ty lli!G;,o ENI l:l'101.c.m,; 11Cfflllll @1 I a I 0 s . ~.IM-ff.A9Hdl· e $ 11© , 3 I ~bl~~ 8 I S • 2 G • ~DIO< 11'9,~ Blat o , ©a , 2 ll TOid l'QAo Chn:i:ttl'lsil • a--e 7 CJ - m~ 0 Ci) I II ' 1 = 4-' ; i!l ~ Ct,u:dl;Jt:=) 1111 IG(w 4.4 Taldty~ C) © 0 I 18 s ~Wll!lb e I I a • 11 Cl ' 0 I 1 0 ·Qwnltlr . Tc:ml~Q,!;j l!rt&"':=~ 19 tll [i) Tarvota 6 . ., a..tllco"-Ullo ® I (j) a a • DlstaflcllDalot>dlM , a a a. 0 • IJ ,.._ OI ""°4 ii }f i Pac,.,latlotl 84nDd llllsD 1CO 0 8 10 I 0 GIi tlDWalo<IIIIIM 10 ID ~ m m ., TcialT~~ 6 115 (!) Ei C!r4 [i) b 45, -'¥J [i} B m B Ii] . 798 " ll!M m 1ri 11. ~ rn B m • rn B m 84.250 l!l 0ffldo °"°. IE e,, 114,350 Cftl! Ollft;lly "' 100 ,...,.1.24 SURFACE WATER ROUTE WORK SHEET O.R. MAX. • • \ CJ;t~\'Jlllf\"'"1 !he 111~ 'llo,,a ~ Moa. Slot. ~,~ pci.0...1 ~· ko,o lkc,,o Go:l<Ofll [il Ol nd~IUU @ e I 0 " •. , ~ ""° IJlfr;;t,I\: 0..:.,.. ;zA2ll,a l!>n QD 1111 " be m ti1 1. ~ 11o o ;. ;,_ 11ft lilM IE . ri B,n,s t:3 <El. o,,c. ... ~ t:, 1:1!:l rn . . m ~ o-...:,..."°""' 11.J El 11,111, l!tlO Cl I 8 8 ' a t&! 3Gi A">" nJ Wt Q ' II a I 0 ~~ G I II • 0 • 8 ' G ' e ~ 1E:IIS ~• Q!!!j'1lChl'bl;)( I kot'I ~ Ill,..,._ u 'f¼ ?91)crW1911t\ 'GI I 12-U 13 I go ~ lliDllll& 11 84 lr1. Ill er caolllisaldlhe ., ' a • I 0 " t;.:.daent Ll:lldUoo ., ' I • ' • . . I TDl&l1~11ccwe • . rn~m-m a[i) ~= Ill~,_ rn·i,yz.ioon~ti,= So"' 0 AIR ~OUT£ WORK SHEET • • GlwOCI ~ ~ lf,oq1 ~•e:tor Aa~.,.,.,.. ~ koro •• "°'· C.C,,cto ~· --· 11c ... C!kc-, OJ ~,-1.'1)(1 ~IC; I'll 0 G ~ 0 Cl& o, l'l ~ f!l b ti. gr:ct.<111 b D>w I!) en-ID t.io.~li}-~ m~~, 8(!) .. 3 0 ' ' 8 Cl.I (.!) C IUalMOt'1 0 ® ' 15 Ill cu ~ ~o Qlwl?.."1$118U:. 0 I I (S') 6 15 • tll.t 'lk>,,1:;11y m i~ID I O.ll ~!loflWh!ll,le 0 , a•©• 4 12 l'lD ~10~ <i), ~I.CftCGIDO R ll 4 0 t2 . Ct11iWtbblllll . I 12 . 10IA' ID'JtU Seo<1 12 @ Iii """ m ;. .:5. ~. m g rn • m a, lino I la 0. r;aulliplJ m I m D rn I 6) 8100 '1.1!00 . m Dt'tld• i;,,. m bJ ,,J#J """' Dlllllip, II)' 1110 il)C .3.85 3 7. t' DIRECT COkTACT WORK SHEET I f • p.,.·D'\11 ll~ ~ e,,,., I ""' "'i'l 'cc'°' Aa~YSI"° ~ ... Ike,,• r.la, ~•. lt,,,cle °"°' ""°' Gcc,,o Ill«_, I]~'" ' • I a ,., m ~~ C-..•tt!O<l&IICI , .. O:ra::lllvUn..:o I) ' I ll ct= \!:ta'IIJ 0 ' • II I • ~, G I I I 1 8 Clu,.1~111, e I I 3 ' I) 11'11!,1 ~I t'.f Hit 0 ' I a I I 8 ' 8 I I o-M, . V~ 1¥n1a ~ l!corll I ~ (al 'I l'll'IJOI I ,., 0.-0 IO Noll/lit! • • a a 4 I • I • Poe: ca,-on ~etoN-ea•ul 0 I I I ' I 8,,141"9 O,,aa,,eo IO S.,,siliwV 0 ' I a I a l;w~ OI ilh8 I\ l u,,ou.. • I I a t ' ~'°" ""'""" 8 t I ' . I t I WIIIRIOolll S-"'91 WolfW" I I t I c • , • .~ .. "-" .... I TD!al To,v.11 &,ec,,1 I• rn fl' ... l,c,IJ 0 a m a [! 1,440 • 6J Oo•oek ,,_ (!) IIJ 1,"0 ...cl -"'P'J l>J MIO Sf(• FIRE ANO EXPLOSION WORK SHEET Documentation for HRS Scorinq of the Statesville FCX Warehoose Ground Water Route Work Sheet l. Observed Release Observed releases -value 45. 2. Route Characteristics a. Depth to aquifer of concern: Not required if release is observed. The calculated approximate depth of the water table below the bottom of the disposal pit is 20 feet. This distance· is only an approximation because the origin al elevation of the grade of the disposal area is unknown, and was estimated. b. Net precipitation: Not required if release is observed. Data is. from the precipitation and evaporation maps provided with the HRS manual. Mean annual precipitation Mean annual lake evap. Net preci pi tat ion -value 2. 52 in -40 in 12 in c. Perrreability of the unsaturated zone: Not required if release is observed. No empirical data exists, but geologic materials observed in the on-site borings were compared to the HRS guidance manual Table 2. The resulting value could be either l or 2, so two HRS scorings were prepared, one using each score. d. Physical state: Not required if release is observed. Powder -value 2 (from interviews with the site manager who was present during disposal). 3. Containment: Not required if release is observed. No 1 iners, containment receives the maximum value -3 -2- 4. Waste Characteristics a. Toxicity/Persistence: Toxicity and Persistence each have a value of 3 for DDT, corrbined in the matrix this receives the maximum value -18 b. Hazardous Waste Quar.tity: From interviews with the site manager who was present during waste disposal, up to 10 tons. This receives a value of 1. 5. Targets a. Ground Water Use: Only incomplete was av a il able . sources exists. information fro'll the Iredell County Heal th Groundwater used and an unthreatened This received a value of 2. ,, b. Distance to nearest well/population served: Again, only limited information was available. Deparbnent municipal The nearest well is less than 2000 feet away at the Carnation Plant next to th FCX warehouse; this well may no longer be in use. This received a score of 4. o,<_ Less than 100 private domestic wells are in the Statesville area. At 3.8 persons per well, this received a score of 2. The matrix score for th is factor was 20. Surface Water Route Work Sheet 1. Observed Release To date no observed releases, and the nearest downstream surface water is over a mile away. value -0 2. Route Characteristics a. Facility Slope and Intervening Terrain: Source for facility slope -Plant blueprint shows an 11 ft. drop over a distance of 416 ft. -This equals a 2.6% slope. e ' -3- Intervening terrain -· USGS toJX) map shows a 130 ft. drop over a distance of one mile. This equals a 2.46% slope. These values cormined in the matrix give a vaue of zero. b. 1-yr, 24 hr. Rainfall: From the map supplied with the HRS guidance manual = 3 in. This receives a value of 2 or 3. Two scores are prepared c. Distance to nearest s_urface water: From the USGS topo map, it is from 1 to 2 miles to the nearest · surface viater. Value 1. d. Physical State -Same as for ground water route -value 2. 3. Containment -Assumes soil contamination, this received a score of 1. 4 Waste Characteristics -same as groundwater route Toxicity/Persistence, score 18, Waste Quantity -score 1 5. Targets -Surface water is not known to be used for drinking, but may be used recreationally -score 2. Air Route No observed releases, air route score is zero. Direct Contact Unless hazardous wastes are found in soil samples, score will be zero. a; Observed Incident Soi 1 s contaminated with pest i ci de. b. Access ib i 1 ity Site is fenced only on three sides -score 3. c. Containment Soil contamination documented -score 15. t -4- d. Waste Characteristics -toxicity Score 3 x 5 = 15 e. Population within one mile Assurres 1000 to 3000 people -score 3.