NCD079044426_20051107_General Electric Co. Shepherd Farm_FRBCERCLA RA_Groundwater Sampling Results Dr. Gary Hill (2002 - 2005)-OCR

www.geotransi tic.corn
Dr. Gary Hill
250 Old TyTy Road
Ti !ion, GA 3 1794-6607
Reference:
Dear Dr. Hill:
Groundwater Sampling Results
June and September 2005
GeoTrans Project No. 2204.100.0 I
I 080 Holcornb 13riclge Ro,1cl
Building I 00, Suite 190
Roswell, Gt\ 30076
770-642-1000 FAX [phone]
November 7, 2005
·--Per your request~the·resultsfrunnhe-recovery and momtormg wells on your property arc
provided. The groundwater was analyzed for seven target volatile organic compounds (VOCs) and three
metals. Note that nitrobenzene and two metals (barium and beryllium) are no longer being sampled for,
this change was approved by the U.S. Environmental Protection Agency (EPA). All field and laboratory
methods utilized were approved by the EPA. The results from March and September 2005 for MW-64,
MW-64A, MW-66 and RWSF-l(see Figure I) are provided in the attached laboratory reports and are
summarized in the attached tables (Table I).
EPA requires General Electric to sample the wells semi-annually as part of a long-term monitoring
plan. Measurements take place in the months of March and September. The next sampling event will
occur in March 2006.
We will continue to report groundwater sampling results to you as they become available. If you
have any questions, please feel free to call me at [phone] or Mr. Barry Hallock at [phone].
cc. Michael Townsend (EPA)
Barry Hallock (GELS)
David Mattison (NCDENR)
P:\GE\DOCS\Resident\Hil\Rcsults\Hill Results! 1-05.tloc
Sincerely,
Staff Scientist
P:\GE\docs\residents\H1ll_site.wor
Explanation
• Site monitor well
♦ Recovery well
Gravel
road
+ Sampled Residential well
0 300
SCALE IN FEET
600
TITLE:
LOCATION:
Location of Shepherd Farm Subsite Features
East Flat Rock, NC
CHECKED PAW ~ ~,g,QTrans, Inc. :;:Trn :~;;;1;·0·
FIGURE:
1
•
•
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results.
Remediation
Parameter Goal
voes (µg/L)
1.2-Dichloroethane
Benzene
Chloroform
cis-1,2-Dichloroethene 70
Tetrachloroethene
trans-1,2-Dichloroethene 70
---·
Trichloroethene 2.8
Vinyl chloride
SVOCs (µg/L)
Nitro benzene 10
METALS TOTAL (µg/L)
Banum
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J -detected, estimated result
UJ -not detected, estimated result
D -dilution sample
E -exceed calibration limit
B -found in blank
NA -not atlalyzed
2000
4
I 5
50
100
MW-64
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0) ND (2.0) ND(2.0) ND(2.0) ND (2.0) ND (2.0)
ND (1.0) ND (I.OJ ND (I.OJ ND (1.0) ND (I.OJ ND (I.OJ
1.0 J ND (2.0J ND (2.0) ND(2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND(2.0J ND (2.0J ND (2.0) ND (2.0)
3.6 2.8 0.83 J 1.9 J 5.0 3.0
ND (2.0) ND (2.0J ND (2.0) ND(20) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0J ND (2.0J ND (2.0J ND (2.0)
ND (I.OJ ND (1.0) ND ( I.OJ ND (1.0) ND(l.O) ND (I.OJ
ND (5.0J ND (5.0) ND (5.5J ND (5.0J ND (5 OJ ND (5.0)
37.9 8 53.0 J 20.1 J 22.0 J 37.9 J 34 5 J
0.68 J 0.68 U 0.51 U 0.75 U 0.67 U 0.45)
1.5 J 12.7 J.4U uu 1.2U 4.7 U
8.4 J 27.7 2.7 UJ 2.7 U 3.4 UJ 7.0 J
5.4 U 0.8 U 1.2 J 0.8 U 0.8 U 0.8 U
Balded values indicate detected concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND(2.0) ND (2.0) ND (2.0)
ND (I.OJ ND (1.0) ND (1.0) ND (1.0)
ND (2.0J ND (2.0J ND (2.0J ND (2.0)
ND(2.0) ND (2.0J ND (2.0) ND (2 0)
0.54 J 1.2 J 4.0 ND (2.0)
ND(2.0J ND(20) ND(20) ND (2.0)
ND (2.0J ND (2.0J ND (2.0J ND (2.0)
ND (1.0) ND ( I.OJ ND(l.OJ ND(l.O)
NA NA ND (5 0) NA
36.8 J 25.6 J 55 5 J 16.8 J
0.22 U 0.26 U 0.26 U 0.26 U
8.8 2.8) 7.9 1.2 U
16.3 J 4. 7 J 16.7 6-4 j
l.5 J I. I U I.I u I.I u --~~---
•
•
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results.
Remediation
Parameter Goal
voes (µg/L)
1.2-Dichloroethane
Benzene
Chlorofonn
cis-1,2-Dichloroethene
Tetrachloroethcne
trans-1,2-Dichloroethcne
Trichloroethene
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene
METALS TOT AL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J -detected, estimated result
UJ -not detected, estimated result
D -dilution sample
E -exceed calibration limit
B -found in blank
NA -not analyzed
70
70
2.8
10
2000
4
15
50
100
MW-64
Mar-03 Jun-03 Sep-03 Mar-04 Sep-04 Mar-OS
ND (2.0J ND (2.0J ND (2.0J ND (2.0) 0.0 0.0
ND (1.0) ND(l.0) ND ( I.OJ ND (1.0) 0.0 0.0
ND(2.0J ND (2.0) ND (2.0) ND (2.0) 0.0 0.0
ND (2.0) ND (2.0) ND(2.0) ND (2.0) 0.0 0.0
ND (2.0) ND(2.0) ND (2.0) ND (2.0) 0.0 0.0
ND (2.0) ND (2.0J ND (2.0J ND (2.0J 0.0 0.0
ND (2.0) ND(2.0J ND (2.0) ND (2.0) 0.0 0.0
ND (I.OJ ND (I.OJ ND (I.OJ ND ( I.OJ 0.0 0.0
NA ND(5.0) 0.0
15.2 J 18.9 J 61.0J 23.2 J 97.5 B
1.4) 0.26 U 0.26 U 0.) U 0.3 U
4.7 U 1.2 U 15.7 4.3 J 12.1 11.7
34) 1.6 J 36.8 8.0 J 37.6 23.0
I. 1 lJ 1.1 lJ 11.0 J 1.1 J 5.8 8 2.5 B
Bolded values indicate detected concentrations greater than remediation goals.
Sep-OS Mar-06 Sep-06 Mar-07
ND(l.0)
ND (1.0)
ND (1.0)
ND(l.O)
0.74 J
ND (I.OJ
ND (I.OJ
ND (1.0)
8.7
19.2
1.8 B
•
•
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Benzene
Chloroform
cis-1,2-Dichloroethene 70
Tetrachloroethene
trans-1,2-Dichloroethene 70
Trichloroe1hene 2.8
Vinyl chloride
SVOCs (µg/L)
Nitro benzene 10
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND • not detected
J -detected, estimated result
UJ -not detected, estimated result
D -dilution sample
E -exceed calibration limit
B -found in blank
NA -not analyzed
2000
4
15
so
100
MW-64A
Sep-00 Dec-00 Mar-01 Jun-01 Sep-OJ Dec-01
ND (2.0J ND (2.0J ND (2.0J ND (2.0J ND (2.0) ND (2.0J
ND(I.OJ ND (1.0) ND (I.OJ ND (I.OJ ND (I.OJ ND (I.OJ
ND(2.0) ND (2.0J ND(2.0J 0.68 J 0.68 J ND (2.0J
ND (2.0J ND (2.0J ND (2.0J ND(2.0J ND (2.0J ND (2.0J
50.2 46.7 43.1 41.8 42.8 41.8
ND (2.0) ND (2.0) ND (2.0J ND (2.0J ND (2.0) ND (2.0)
ND(2.0J ND (2.0) ND (2.0) ND (2.0J ND (2.0J ND (2.0J
ND (I.OJ ND (I.OJ ND (1.0) ND (I.OJ ND (I.OJ ND ( I.OJ
ND (5.0J ND (5.0J ND (5 0) ND (5.0J ND (5.0) ND (5.0J
34.0J 33.6 J 360J 32. 7 J 29.7 J 30.2 J
0.79 U 0.86 UJ 0.76 U 0.83 U 0.6 U 0.22 U
1.2 u 1.7 UJ 2.5 U 1.4 U 1.2 J 4.4 U
90.7 76.9 J 92.4 J 70.8 51.4 J 50.4
1.9 lJ 0.8 UJ 0.97 J 0.8 U 0.8 U 0.8 U
Bolded values indicate detected concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0J ND (2.0J ND (2.0) ND (2.0)
ND(I.OJ ND (I.OJ ND (I.OJ ND (I.OJ
0.77 J 0.75 J 0.74 J 0.8 J
ND (2.0J ND(2.0J ND(2.0J ND (2.0J
43.8 37.2 36.3 29.5
ND(2.0J ND (2.0J ND (2.0) ND (2.0)
ND (2.0J ND (2.0J ND (2.0J ND(2.0J
ND (I.OJ ND (I.OJ ND (I.OJ ND(I.OJ
NA NA NIJ(5.0) NA
31.8 J 32.1 J 32.4 J 42.8 J
0.22 U 0.26 U 0.26 U 0.26 U
-----·
2.7 J 1.2 u 1.8 U 1.2 lJ
54.0 J 93.4 99.5 216
0.8 U I.I u I.I u I.I u
•
•
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Benzene
Chloroform
cis-1,2-Dichlorncthcne 70
Tt:trachloroethene
trans-1,2-Dichloroethene 70
Trichloroethene 2.8
Vinyl chloride
SVOCs (µg/L)
Nitroben7,cnc 10
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J -detected, estimated result
UJ -not detected, estimated result
D -dilution sample
E • exceed calibration limit
B -found in blank
NA -not analyzed
2000
4
IS
50
100
MW-64A
Mar-03 Jun-03 Sep-03 Mar-04 Sep-04 Mar-05 Sep-OS Mar-06 Sep-06 Mar-07
ND (2.0) ND (2.0) ND (2.0) ND (2.0) 0.0 0.0 ND (LO)
ND (1.0) ND(l.O) ND (1.0) ND (1.0) 0.0 0.0 ND (1.0)
0.65 J 0.63 J 0.51 J 0.66 J 0.65 J 0.57 J 0.56 J
ND (2.0) ND (2.0) ND (2.0) ND (2.0) 0.0 0.0 ND (1.0)
34.9 33.7 38.0 40.9 41.7 36.2 45.7
ND (2.0) ND (2.0) ND (2.0) ND (2.0) 0.0 0.0 ND (1.0)
ND (2.0) ND (2.0) ND(2.0) ND (2.0) 0.0 0.0 0.55 J
ND (I.OJ ND (1.0) ND (1.0) ND (LO) 0.0 00 ND(l.O)
NA ND (5.0) 0.0
35.7 J 36.8 J 37.4 J 35.6 J 3348
0.26 U 0.26 U 0.26 U 0.3 U 0.3 U
1.3 u 1.2 U 1.2 U 1.2 J 1.2 u 1.2 U 1.2 u
137 264 167 126 81.5 72.5 91.2
1.1 u 1.1 u 1.1 u 1.1 u I.JU 1.1 u 10.7 B
-----------------------------------------
Bolded values indicate dctt:cted concentrations greater than remediation goals.
•
•
Table 1. Shepherd Farm Subsite • Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1.2-Dichlorocthane
Benzene
Chloroform
cis-1.2-Dichloroethenc 70
Tetrachloroethcne
trans-1.2-Dichloroethene 70
Trichloroethenc 28
Vinyl chloride
SVOCs (µg/L)
Nitro benzene 10
METALS TOTAL (µg/L)
Barium
Beryllium
----·--
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J -detected, estimated result
UJ -not detected, estimated result
D -dilution sample
E -exceed calibration limit
B -found in blank
NA -not analyzed
2000
4
15
50
100
MW-66
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0) ND(2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND(l.0) ND (1.0) ND (1.0) ND(l.0)
ND (2.0) ND (2.0) 0.81 J ND (2.0) 0.77 J ND (2.0)
1.6 J ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
23.2 J 45.8 53.4 54.5 65.7 58.5
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
0.94 J ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND(l.0) ND ( 1.0) ND (l.0) ND (1.0)
ND(50) ND (5.0J ND (5.5) ND (5.0) ND(S0) ND (5.0)
52.3 J 36.1 J 39_6 J 26.0 J 40.0 J 39.2 J
1.5 u 0.87 UJ 0.8 U 0.94 U 0.81 U 022U
4.2 J 1.6 UJ 3.8 U 1.6 U 1.9 J 6.3 U
223 57.3 J 81.2 20.4 119.0 .I 98.9
5.3 U 1.8 J 1.8 U 0.8 U 1.2 J 1.9 J
Balded values indicate detected concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND(2.0) ND(2.0) ND (2.0)
ND (1.0) ND ( 1.0) ND (1.0) ND ( 1.0)
0.85 J 0.65 J 0.69 J 0.7 J
ND (2.0) 0.52 J 0.55 J ND (2.0)
61.1 64.8 71.3 76.6
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND(2.0J ND (2.0)
ND (1.0) ND(l.0) ND (1.0) ND(l.0)
NA NA ND (5.0) NA
28.0 J 26.5 J 30.8 J 28.9 J
0.22 U 0.26 U 0.26 U 0.26 U
2.5 J 1.2 U 2.5 U 1.2 U
16.4 J 25.9 45.0 38.8
0.8 U I.I u I. I U I.I lJ
•
•
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Bcnzem:
Chlorofonn
cis-1,2-Dichloroethene
Tetrachloroethene
trans-1,2-Dichloroethene
Trichloroethenc
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J -detected, estimated result
UJ -not detected, estimated result
D -dilution sample
E • exceed calibration limit
B -found in blank
NA -not analyzed
70
70
2.8
10
2000
4
15
50
100
MW-66
Mar-03 Jun-03 Sep-03 Mar-04 Sep-04 Mar-05
ND (2.0) ND(2.0) ND (2.0) ND (2.0) 0.0 0.0
ND (1.0) ND ( I.OJ ND(l.0) ND(l.0) 0.0 0.0
0.66 J 0.59 J 0.69 J ND (2 OJ 0.0 0.0
0.89 J 0.791 0.97 J 0.81 J 1.0 J 0.7 J
80.2 83.0 76.6 80.4 82.1 69.4
ND (2.0J ND (2.0J ND (2.0J ND(2.0) 0.0 0.0
ND (2.0J ND (2.0J ND (2.0J ND (2.0) 0.0 0.0
ND (I.OJ ND (I.OJ ND (JO) ND (I.OJ 0.0 0.0
NA ND (5.0J 0.0
22.5 J 22.8 J 22.7 J 24.6 J 23.6 B
0.26 lJ 0.26 U 0.26 U 0.3 U 0.3 U
l.4U 1.2 U 1.2 U 1.3 J 1.2 U 2.9 B
6.6 J 14.1 J 5.9 J 4.5 J 15.9 8.5 B
JIU I.I u I.I u I.I u I.I u I.I u
Balded values indicate detected concentrations greater than remediation goals.
Sep705 Mar-06 Sep-06 Mar-07
ND (I.OJ
ND(l.0)
ND (I.OJ
0.59 J
50.9
ND (I.OJ
ND(l.0)
ND(l.0)
4.4 B
18.9
I.I U
•
•
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethanc
Benzene
Chloroform
cis-1,2-Dichloroethenc 70
Tetrachloroethcne
trans-1,2-Dichloroethene 70
Trichlorocthenc 2.8
Vinyl chloride
SVOCs (µg/L)
Nitrohcnzene 10
METALS TOTAL (µg/L)
Barium
Bel)'llium
---------·
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J -detected, estimated result
UJ • not detected, estimated result
D -dilution sample
E • exceed calibration limit
B -found in blank
NA -not analyzed
2000
4
15
50
100
RWSF-1
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0) ND (2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0)
ND(l.0) ND(l.0) ND(l.0) ND(l.0) ND (1.0) ND(l.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
34.0 51.4 43.2 40.4 46.3 52.6
ND (2.0) ND (2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0)
ND (I.OJ ND (I.OJ ND (1.0) ND(l.0) ND (1.0) ND (1.0)
ND (5.0) ND (5.0) ND (5.5) ND (5.5) ND (5.0) ND (5.0)
I 61.0 J 193.0 J 290 242.0 254.0 J 153.0 J
0.3 U 2.6 UJ 2.2 U 2.3 U I. I J 1.2 J
1.5 J 50.6 J 49.5 21.4 24.3 10.4 U
65.6 42.6 J 109.0 J 100.0 90.1 J 71.8 J
13.7 J 1.4 J 6.5 J 0.8 U 3.5 J 1.8 J
Bolded values indicate detected concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND(20) ND (2.0) ND(2.0i
ND(l.0) ND (1.0) ND (1.0) ND (1.0)
0.52 J ND(2.0) 0.52 J ND (2.0)
ND (20) ND (2.0) ND(2.0) ND (2.0)
56.3 56.4 43.2 63.6
ND (2.0) ND (2.0) ND(2.0) ND(2.0)
ND (2.0) ND(2.0) ND(20) ND(2.0)
ND (1.0) ND (1.0) ND (I.OJ ND(l.O)
NA NA ND (5 0) NA
156.0 J 142.0 J 134.0J 61.3 J
0.22 U 0.26 U 0 26 lJ 0.26 U
26.1 22.7 18.4 1.2 U
98.1 J 105 77.6 0.16 lJ
4.2 J 11 U I.I 1J I. I U
•
•
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1.2-Dichloroethane
Benzene
Chloroform
cis-1,2-Dichloroethene 70
Tetrachloroethene
trans-1,2-Dichloroethenc 70
Trichloroethene 28
Vinyl chloride
SVOCs (µg/L)
Nitrobel17..cne 10
METALS TOTAL (µg/L)
Rarium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J • detected, estimated result
UJ -not detected, estimated result
D • dilution sample
E -exceed calibration limit
B -found in blank
NA -not analyzed
2000
4
I 5
50
JOO
RWSF-1
Mar-03 Jun-03 Sep-03 Mar-04 Sep-04 Mar-05
ND (2.0) ND (2.0) ND (2.0J ND (2.0J 0.0 0.0
ND ( I.OJ ND ( I.OJ ND (1.0) ND (I.OJ 0.0 0.0
ND (2.0) ND (2.0J ND (2.0) ND(2.0) 0.0 0.0
ND (2.0J ND (2.0J 3.5 ND(2.0J 0.0 0.0
32.2 38.1 37.7 44.3 36.8 51.6
ND (2.0) ND (2.0J ND (2.0J ND (2.0J 0.0 0.0
ND (2.0J ND (2.0J 0.91 J ND(2.0J 0.0 0.0
ND (I.OJ ND (I.OJ ND (1.0) ND (1.0) 0.0 0.0
NA ND (5.0) 0.0
28.3 J 47.6 J I 52.0 J 141.0J 132.0 B
0.26 U 0.26 U 0.26 U 0.3 U 0.3 U
30.5 106 7.9 14.0 13.8 14.5
12.8 J 126 64.5 55.7 106 152
311 100.0 1.8 J 40.8 J 10.7 8 21.4 B
Boldcd values indicate detected concentrations greater than remediation goals
Sep-05 Mar-06 Sep-06 Mar-07
ND (I.OJ
ND (1.0)
ND(I.O)
0.54 J
69.9
ND (I.OJ
ND(I.OJ
ND (1.0)
17.0
97.3
8.5 B
• •
"'
Accutest Laboratories "'
Report of Analysis Page l of l
Client Sample ID:
Lab Sample ID:
Matrix:
MW-64
F35307-6
AQ -Ground Water
SW846 8260B . rvt_et!iod: _
Project: GELS: East Flat Rock, NC
File ID OF Analyzed
Run #1 ]018420.D 10/10/05
Run #2
IRun #1
Purge Volume
5.0 ml
Run #2
CAS No. Compound Result
71-43-2 Benzene ND
67-66-3 Chloroform ND
107-06-2 1,2-Dichloroethane ND
156-59-2 cis-1,2-Dichlorocthylene ND
156-60-5 trans-1,2-Dichloroethylene ND
127-18-4 Telrachlorocthylene 0.74
79-01-6 Trichloroethylene ND
75-01-4 Vinyl chloride ND
CAS No. Surrogate Recoveries Run# l
1868-53-7 Dibromofluoromcthane 102%
17060-07-0 1,2-Dichloroethane-D4 107%
2037-26-5 Toluene-OS 99%
460-00-4 4-Bromofluorobenzene 108%
By
MM
RL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Run# 2
Date Sampled: 09/27/05
Date Received: 09/29/05
Percent Solids:_ n/a _
Prep Date Prep Batch
n/a n/a
MDL Units Q
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1 J
0.50 ug/1
0.50 ug/1
Limits
86-115%
73-126%
86-112%
83-119%
Analytical Balch
VJ760
ND = Not detected MDL -Method Detection Limit ] = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
tlffll!I 15 of 71
g:]ACC:UTEE.iT.
FJ5J07 : ' :, ·
•
Accutest Laboratories
Client Sample JD: MW-64
Lab Sample ID: F35307-6
Matrix: AQ -Ground Water
•
Report of Analysis
Date Sampled: 09/27/05
Date Received: 09/29/05
Percent Solids: n/a
Page I of I
Project: GELS: East Flat Rock, NC
Metals Analysis
Analyte
Lead
Manganese
Nickel
Result
8.7
19.2
1.8 B
RL
5.0
15
40
(I) Instrument QC Batch: MA4594
(2) Prep QC Batch: MP8681
RL = Reporting Limit
MDL = Method Detection Limit
MDL Units
12 ug/1
0.20 ug/1
I. I ug/1
OF Prep Analyzed By Method Prep Method
09/30/05 10/03/05 RS SW846 60!08 1 SW846 30 I OA 2
09/30/05 10/03/05 RS SW846 60 I OB I SW846 30 I 0A 2
09/30/05 10/03/05 RS SW846 6010B I SW846 3010A 2
· --· u· = ·Indicales a-result_<_MDL
B = Indicates a result > = MDL but < RL
~!!'.I 16 of 71
E;i~T.
F35307
• •
Accutest Laboratories
Report of Analysis Page l of l
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
MW-64A
F35307-7
AQ -Ground Water
SW846 8260B
Project: GELS; East Flat Rock, NC
File ID OF Analyzed
Run #1 ]018435.D 10/11/05
Run #2
!Run #1
Purge Volume
5.0 ml
Run #2
CAS No. Compound Result
71-43-2 Benzene ND
67-66-3 Chloroform 0.56
107-06-2 1,2-Dichloroethane ND
l 56-59-2 cis-1,2-Dichloroethylene ND
156-60-5 trans-1,2-Dichloroethylene ND
127-18-4 Tetrachlorocthylene 45.7
79-01-6 Trichloroethylene 0.55
75-01-4 Vinyl chloride ND
CAS No. Sunogate Recoveries Run# l
1868-53-7 Dibromofluoromethane 104%
17060-07-0 l, 2-Dichloroethane-O4 113%
2037-26-5 Toluene-O8 100%
460-00-4 4-Bromofluorobenzene 109%
By
MM
RL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Run# 2
Date Sampled: 09/27/05
Date Received: 09/29/05
Percent Solids: n/a
Prep Date Prep Batch
n/a n/a
MDL Units Q
0.50 ug/1
0.50 ug/1 J
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1 J
0.50 ug/1
Limits
86-1!5%
73-126%
86-112%
83-119%
Analytical Batch
VJ761
ND -Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL -Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
l;llll!'.i 17 of 71
[,j ~:r.
F35307
•
Accutest Laboratories
Client Sample ID:
Lab Sample ID:
Matrix:
MW-64A
F35307-7
AQ -Ground Water
Report of Analysis
Date Sampled: 09/27 /05
Date Received: 09/29/05
Percent Solids: n/a
Page I of I
Project: GELS: East Flat Rock, NC
Metals Analysis
Analyte Result RL
Lead 1.2 U 5.0
Manganese 91.2 15
Nickel 10.7 B 40
(I) Instrument QC Batch: MA4594
(2) Prep QC Batch: MP8681
RL ~ Reporting Limit
MDL = Method Detection Limit
MDL
1.2
0.20
I.I
Units DF Prep Analyzed By Method Prep Method
ug/1 09/30/05 10/03/05 RS SW846 60l0B I SW846 3010A 2
ug/1 09/30/05 10/03/05 RS SW8'16 60 I OB I SW846 30IOA 2
ug/1 09/30/05 10/03/05 RS SW846 6010B 1 SW846 30IOA 2
U = Indicates a result < MDL
B = Indicates a result > = MDL but < RL
• •
Accutest Laboratories
Report of Analysis Page I of I
Client Sample ID: MW-66
Lab Sample ID: F35307-l 7 Date Sampled: 09/28/05
Matrix: AQ -Ground Water Date Received: 09/29/05
Method: SW846 8260B Percent Solids: n/a
Project: GELS; East Flat Rock, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #I M0007876.D 10/11/05 KK n/a n/a VM337
Run #2
IRun #I
Purge Volume
5.0 ml
Run #2
CAS No. Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 0.50 ug/1
67-66-3 Chloroform ND 1.0 0.50 ug/1
107-06-2 1,2-Dichloroethane ND 1.0 0.50 ug/1
156-59-2 cis-1,2-Dichloroethylene 0.59 1.0 0.50 ug/1 J 156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.50 ug/1
127-18-4 Tetrachloroethylene 50.9 1.0 0.50 ug/1
79-01-6 Trichloroethylene ND 1.0 0.50 ug/1
75-01-4 Vinyl chloride ND 1.0 0.50 ug/1
CAS No. Surrogate Recoveries Run# I Run# 2 Limits
1868-53-7 Dibromufluoromethane 99% 86-115%
17060-07-0 I, 2-Dichloroethane-D4 99% 73-126%
2037-26-5 Toluene-D8 101% 86-112%
460-00-4 4-Bromofluorobcnzene 101% 83-119%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analytc found in associated method blank
N = Indicates presumptive evidence of a compound
!.'llll!I 35 of 71
gjACCUTEST._ ·-····•·"·"' ···••-,·-········ FJ5J07
•
Accutest Laboratories
Client Sample ID: MW-66
Lab Sample ID: F35307-17
Matrix: AQ -Ground Water
Report of Analysis
Date Sampled: 09/28/05
Date Received: 09/29/05
Percent.Solids:_ n/a_
Project: GELS; East Flat Rock, NC
Metals Analysis
Analyte Result RL
Lead 4.4 B 5.0
Manganese 18.9 15
Nickel I.I u 40
(I) Instrument QC Batch: MA4596
(2) Prep QC Batch: MP8687
MDL
1.2
0.20
I. I
Units DF Prep Analyzed By Method
ug/1 10/03/05 10/04/05 OM SW846 60l0B 1
ug/1 l0/03/05 10/04/05 OM SW846 60tOB 1
ug/1 l0/03/05 l0/04/05 OM SW846 60l0B I
Page I of I
Prep Method
SW846 30 I OA 2
SW846 30 I OA 2
SW846 30 IOA 2
--Rh-=-Rej,orting-1::imit-----------------u--=-Indlcaten-result<-MD,-------
MDL = Method Detection Limit B = Indicates a result > = MDL but < RL
f.'!lll!'.I 3 6 of 71
~ACClJ"Tl:ST.
F35J07
• •
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: RWSF-1
Lab Sample ID: F35307-18 Date Sampled: 09/28/05
Matrix: AQ -Ground Water Date Received: 09/29/05
Method: SW846 8260B. ---Percent Solids: n/a ..
Project: GELS; East Flat Rock, NC
File ID OF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 M0007877.D 10/11/05 KK n/a n/a VM337
Run #2
!Run #1
Purge Volume
5.0 ml
Run #2
CAS No. Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 0.50 ug/1
67-66:f Ctiforoform ND ___ 1.0 0.50 ug/1
107-06-2 1,2-Dichloroethane ND 1.0 0.50 ug/1
156-59-2 cis-1,2-Dichloroethylene 0.54 1.0 0.50 ug/1 J
156-60-5 lrans-1,2-Dichloroethylene ND 1.0 0.50 ug/1
127-18-4 Tetrachloroethylene 69.9 1.0 0.50 ug/1
79-01-6 Trichloroethylene ND 1.0 0.50 ug/1
75-01-4 Vinyl chloride ND 1.0 0.50 ug/1
CAS No. Surrogate Recoveries Run# l Run# 2 Limits
1868-53-7 Dibromofluoromethane 100% 86-115%
17060-07-0 l ,2-Dichloroethane-D4 100% 73-126%
2037-26-5 Toluene-OS 100% 86-112%
460-00-4 4-Bromofluorobcnzene 96% 83-119%
ND = Not detected MDL -Method Detection Limit J == Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presl!-mptive evidence of a compound
fllJJl!'.I _ 37 of71
E:iACCUTEST. ............. , ....... , ............ ,.,,
FJ5J07
•
Accutest Laboratories
Client Sample ID:
Lab Sample ID:
Matrix:
RWSF-1
F35307-18
AQ -Ground Water
•
Report of Analysis
Date Sampled: 09/28/05
Date Received: 09/29/05
Percent Solids:-n/a--..
Page 1 of 1
Project: GELS; East Flat Rock, NC
Metals Analysis
Analyte Result RL MDL
Lead 17.0 5.0 1.2
Manganese 97.3 15 0.20
Nickel 8.5 B 40 1.1
(1) Instrument QC Batch: MA4596
(2) Prep QC Batch: MP8687
t -Reporling-ttrnl
MDL = Method Detection Limit
Units DF
ug/1
ug/1
ug/1
Prep Analyzed By Method
10/03/05 10/04/05 DM SW846 60IOB 1
10/03/05 10/04/05 DM SW846 60108 1
10/03/05 10/04/05 DM SW846 6010B 1
· --=Inditates-aresult-<MD
Prep Method
SW846 3010A 2
S\V846 3010A 2
SW846 30 I OA 2
B = Indicates a result > = MDL but < RL
fllll!) 38 of 1 __ 1 __ E;"jACCUTEST. ....... , .. , .. ,, .. , .,,,,, F35307 : ':• ,· · 0 ; ,. • ',. '
• •
Accutest Laboratories
Report of Analysis Page 1 of I
Client Sample ID: WW-5
Lab Sample ID: F35340-l
Matrix: AQ -Ground Water
Method: SW846 82608
Project: GELS; East Flat Rock, NC
Run #I
Run #2
!Run #1
Run #2
CAS No.
71-43-2
67-66-3
107-06-2
156-59-2
156-60-5
127-18-4
79-01-6
75-01-4
CAS No.
1868-53-7
17060-07-0
2037-26-5
460-00-4
File ID
M0007878.D
Purge Volume
5.0 ml
Compound
Benzene
Chloroform
DF
I
1,2-Dichloroethane
cis-1, 2-Dichloroethylene
trans-1,2-Dichloroethylene
Tetrachloroethylene
Trichloroethylene
Vinyl chloride
Surrogate Recoveries
Dibromonuoromethane
1,2-Dichloroethane-D4
Toluene-DB
4•Bromofluorobenzene
Analyzed
10/11/05
Result
ND
ND
ND
ND
ND
ND
ND
ND
Run# 1
101%
98%
100%
102%
Date Sampled: 09/28/05
Date Received: 09/30/05
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch KK n/a n/a VM337
RL MDL Units Q
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
Run# 2 Limits
86-115%
73-126%
86-112%
83-119%
ND = Not detected MDL · Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
1111!'.1 4 of 22
lg ACCU I ES I.
FJSJ-10
• •
"'
Accutest Laboratories
Report of Analysis Page I of I
Client Sample ID: WW-5
Lab Sample ID: F35340-I
Matrix: AQ -Ground Water
Project: GELS; East Fial Rock, NC
Metals Analysis
Analyte Result RL
Lead 10.7 5.0
Manganese 109 15
Nickel I.I u 40
(I) Instrument QC Balch: MA4596
(2) Prep QC Balch: MP8687
RL = Reporting Limit
MDL = Method Detection Limit
MDL Units
1.2 ug/1
0.20 ug/1
I.I ug/1
DF
I
I
I
Prep
Date Sampled: 09/28/05
Date Received: 09/30/05
Percent Solids: n/a
Analyzed By Method
10/03/05 10/04/05 DM SW846 60!0B I
10/03/05 10/04/05 DM SW846 60!0B t
10/03/05 10/04/05 DM SW846 60!0B I
U = Indicates a result < MDL
Prep Method
SW846 3010A 2
SWB46 3010A 2
SW846 3010A 2
B = Indicates a result > = MDL but < RL
1!111!'.1 5 of 22
l;iACCUIESi.
FJ5340
•
Accutest Laboratories
Report of Analysis Page I of I II
Client Sample ID: WW-82
Lab Sample ID: F35340-2 Date Sampled: 09/28/05
Matrix: AQ -Ground Water Date Received: 09/30/05
Method: SW846 8260B Percent Solids: n/a
Project: GELS; East Flat Rock, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #I M0007879.D 10/11/05 KK n/a n/a VM337
Run #2
IRun #I
Purge Volume
5.0 ml
Run #2
CAS No. Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 0.50 ug/1
67-66-3 Chloroform ND 1.0 0.50 ugn
107-06-2 1,2-Dichloroethane ND 1.0 0.50 ug/1
156-59-2 cis-1, 2-Dichloroethylene ND 1.0 0.50 ug/1
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.50 ug/1
127-18-4 Tetrachloroethylene ND 1.0 0.50 ug/1
79-01-6 Trichloroethylene ND 1.0 0.50 ug/1
75-01-4 Vinyl chloride ND 1.0 0.50 ugn
CAS No. Surrogate Recoveries Run# I Run# 2 Limits
1868-53-7 Dibromonuoromethane 99% 86-115%
17060-07-0 1,2-Dichloroethane-D4 98% 73-126%
2037-26-5 Toluene-OS 100% 86-112%
460-00-4 4-Bromonuorobenzene IOI% 83-II9%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
111!'1 6 of 22
CiACO I I ES J.
FJSJ.JO
•
Accutest Laboratories
Client Sample ID:
Lab Sample ID:
Matrix:
WW-82
F35340-2
AQ -Ground Water
•
Report of Analysis
Date Sampled: 09/28/05
Date Received: 09/30/05
Percent Solids: n/a
Page I of I
Project: GELS; East Flat Rock, NC
Metals Analysis
Analyte Result RL
Lead 8.8 5.0
Manganese 1090 15
Nickel 7.5 B 40
(I) Instrument QC Batch: MA4600
(2) Prep QC Batch: MP8694
RL = Reporting Limit
MDL = Method Detection Limit
MDL Units
1.2 ug/1
0.20 ug/1
I.I ug/1
DF
I
I
I
Prep Analyzed By Method Prep Method
10/04/05 10/05/05 DM SW846 60 I OB I SW846 3010A 2
10/04/05 10/05/05 DM SWB46 60108 I SWB46 3010A 2
10/04/05 10/05/05 DM SW846 60108 I SW846 3010A 2
U = Indicates a result < MDL
B = Indicates a result > = MDL but < RL
1111!1 7 of 22
11:i!ACCUIESI.
FJ5J40
• •
Accutest Laboratories
Report of Analysis Page I of I IZ
Client Sample ID: WW-28
Lab Sample ID:. F35340-3 Date Sampled: 09/28/05
Matrix: AQ -Ground Waler Date Received: 09/30/05
Method: SW846 82608 Percent Solids: n/a
Project: GELS: East Flat Rock. NC
File ID OF Analyzed By Prep Date Prep Batch Analytical Batch
Run #I M0007880.D I I 0/11/05 KK n/a n/a VM337
Run #2
IRun #I
Purge Volume
5.0 ml
Run #2
CAS No. Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 0.50 ug/1
67-66-3 Chloroform ND 1.0 0.50 ug/1
107-06-2 1,2-Dichloroelhane ND 1.0 0.50 ug/1
156-59-2 cis-1,2-DicWoroethylene ND 1.0 0.50 ug/1
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.50 ug/1
127-18-4 TetracWoroethylene ND 1.0 0.50 ug/1
79-01-6 Trichloroethylene ND 1.0 0.50 ug/1
75-01-4 Vinyl chloride ND 1.0 0.50 ug/1
CASNo. Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100% 86-115%
17060-07-0 1,2-Dichloroelhane-D4 99% 73-126%
2037-26-5 Toluene-OS 100% 86-112%
460-00-4 4-Bromofluorobenzene 101% 83-119%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
1111!1 8 of 22
11.j ACCI I I ES I.
FJ5J40
•
Accutest Laboratories
Client Sample ID:
Lab Sample ID:
Matrix:
WW-28
F35340-3
AQ -Ground Water
Report of Analysis
Date Sampled: 09/28/05
Date Received: 09/30/05
Percent Solids: n/a
Page I of I
Project: GELS; East Flat Rock, NC
Metals Analysis
Analyte Result RL
Lead 8.5 5.0
Manganese 23.2 15
Nickel 1.IU 40
(I) Instrument QC Batch: MA4600
(2) Prep QC Batch: MP8694
RL = Reporting Limil
MDL = Method Detection Limil
MDL
1.2
0.20
I.I
Units DF
ug/1
ug/1
ug/1
Prep Analyzed By Method Prep Method
10/04/05 10105/05 DM SW846 60108 I SW846 30IOA 2
10/04/05 10/05/05 DM SW846 60108 I SW846 30IOA 2
10/04/05 10/05/05 DM SW846 60 I OB I SW846 30IOA 2
U = Indicates a result < MDL
B = Indicates a result > = MDL but < RL
1111!'.1 9 of 22
l.3ACCUIESI.
FJSJW
•
Accutest Laboratories
Report of Analysis Page I of I II
Client Sample ID: WW-17
Lab Sample ID: F35340-4
Matrix: AQ -Ground Water
Method: SW846 8260B
Project: GELS: East Flat Rock, NC
Run #I
Run #2
IRun #I
Run #2
CAS No.
71-43-2
67-66-3
107-06-2
156-59-2
156-60-5
127-18-4
79-01-6
75-01-4
CAS No.
1868-53-7
17060-07-0
2037-26-5
460-00-4
File ID
M000788I.D
Purge Volume
5.0 ml
Compound
Benzene
Chlorofonn
DF
I
1,2-Dichloroethane
cis-1,2-Dichloroethylene
trans-I, 2-Dichloroethylene
Tetrachloroethylene
Trichloroethylene
Vinyl chloride
Surrogate Recoveries
Dibromofluoromethane
I ,2-Dichloroethane-D4
Toluene-DH
4-Bromofluorobenzene
Analyzed
10/12/05
Result
ND
ND
ND
ND
ND
1.5
ND
ND
Run# I
98%
99%
101%
99%
Date Sampled: 09/28/05
Date Received: 09/30/05
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
KK n/a n/a VM337
RL MDL Units Q
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
Run# 2 Limits
86-115%
73-126%
86-112%
83-119%
ND = Not detected MDL -Method Detection Limil J = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
11!111!'.1 1 o of 22
;iACCU I ES I.
F35340
•
Accutest Laboratories
Client Sample ID:
Lab Sample ID:
Matrix:
WW-17
F35340-4
AQ -Ground Water
•
Report of Analysis
Date Sampled: 09/28/05
Date Received: 09/30/05
Percent Solids: n/a
Page I of I
Project: GELS: East Flat Rock, NC
Metals Analysis
Analyte Result RL
Lead 2.1 B 5.0
Maogaoese 95.9 15
Nickel I.I u 40
(I) Instrument QC Batch: MA4600
(2) Prep QC Batch: MP8694
RL = Reporting Limit
MDL = Method Detection Limit
MDL
1.2
0.20
I.I
Units DF
ug/1
ug/1
ug/1
Prep Analyzed By Method Prep Method
10/04/05 10/05/05 DM SW846 60IOB I SW846 30IOA 2
10/04/05 10/05/05 DM SW846 6010B 1 SW846 3010A 2
10/04/05 10/05/05 DM SW846 60 I OB I SW846 3010A 2
U = Indicates a result < MDL
B = Indicates a result > = MDL but < RL
1111!1 11 of 22 Iii ACX:U I ES I.
FJSJIIO
• •
"' Accutest Laboratories (J1
Report of Analysis Page I of I
Client Sample ID: WW-73
Lab Sample ID: F35340-5 Date Sampled: 09/29/05
Matrix: AQ -Ground Water Date Received: 09/30/05
Method: SW846 8260B Percent Solids: n/a
Project: GELS; East Flat Rock, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #I M0007882.D I I0/12/05 KK n/a n/a VM337
Run #2
!Run #I
Purge Volume
:Run #2
5.0 ml
CAS No. Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 0.50 ug/1
67-66-3 Chloroform ND 1.0 0.50 ug/1
107-06-2 1,2-Dichloroethane ND 1.0 0.50 ug/1
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.50 ug/1
156-60-5 trans-I , 2-Dichloroethylene ND 1.0 0.50 ug/1
127-18-4 Tetrachloroethylene ND 1.0 0.50 ug/1
79-01-6 Trichloroethylene ND 1.0 0.50 ug/1
75-01-4 Vinyl chloride ND 1.0 0.50 ug/1
CAS No. Surrogate Recoveries Run# I Run# 2 Limits
1868-53-7 Dibromofluoromethane 98% 86-115%
17060-07-0 J ,2-Dichloroethane-D4 100% 73-126%
2037-26-5 Toluene-DB IOI% 86-112%
460-00-4 4-Bromofluorobenzene 100% 83-119%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
llilll!I 12 of 22 c:i ACC.U i ES I.
FJS340
•
Acculesl Laboralories
Client Sample ID:
Lab Sam pie ID:
Matrix:
WW-73
F35340-5
AQ -Ground Water
Report of Analysis
Dale Sampled: 09/29/05
Date Received: 09/30/05
Percent Solids: n/a
Page I of I
" CJ"
Project: GELS; Easl Fla! Rock. NC
Metals Analysis
Analyte Result RL
Lead 4.8 B 5.0
Manganese 12.5 B 15
Nickel 4.2 B 40
(I) lnslrumenl QC Balch: MA4600
(2) Prep QC Balch: MPB694
RL = Reporting Limit
MDL = Method Deleclion Limil
MDL
1.2
0.20
1.1
Units DF
ug/1
ug/1
ug/1
Prep Analyzed By Method Prep Method
10/04/05 10/05/05 DM SW846 60108 I SW846 3010A 2
10/04/05 10/05/05 DM SW846 60108 I SW846 30 I 0A 2
10/04/05 10/05/05 DM SW846 60108 I SW846 3010A 2
U = Indicales a result < MDL
B = Indicales a resull > = MDL but < RL
111!'.1 13 of 22 riiAC.X:U I ESI.
FJS340
•
"'
Accutest Laboratories i:r.
Report of Analysis Page 1 of 1
Client Sample ID: WW-34
Lab Sample ID: F35340-6
Matrix: AQ • Ground Water
Method: SW846 82608
Project: GELS; East Flat Rock, NC
Run #1
Run #2
IRun #1
Run #2
CAS No.
71-43-2
67-66-3
107-06-2
156-59-2
156-60-5
127-18-4
79-01-6
75-01-4
CAS No.
1868-53-7
17060-07-0
2037-26-5
460-00-4
File ID
M0007894.D
Purge Volume
5.0 ml
Compound
Benzene
Chloroform
DF
1
1,2-Dichloroethane
cis-1,2-Dichloroethylene
trans-1,2-Dichloroethylene
Tetrachloroethylene
Trichloroethylene
Vinyl chloride
Surrogate Recoveries
Dibromofluoromethane
1,2-Dichloroethane-D4
Toiuene-D8
4-Bromofluorobenzene
Analyzed
10/12/05
Result
ND
ND
ND
ND
ND
ND
ND
ND
Run# 1
98%
99%
100%
99%
ND = Not detected MDL • Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range
Date Sampled: 09/28/05
Date Received: 09/30/05
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
KK n/a n/a VM338
RL MDL Units Q
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
Run# 2 Limits
86-115%
73-126%
86-112%
83-119%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
11!111!'.1 14 of 22 Ci ACCU I ES I,
FJSJ'10
•
Accutesl Laboratories
Client Sample ID:
Lab Sample ID:
Matrix:
WW-34
F35340-6
AQ -Ground Waler
•
Report of Analysis
Date Sampled: 09/28105
Date Received: 09/30/05
Percent Solids: n/a
Page I of I
Project: GELS; Easl Flat Rock, NC
Metals Analysis
Analyte Result RL
Lead 2.5 B 5.0
Manganese 5.2 B 15
Nickel 1.1 u 40
(I) Instrument QC Balch: MA4600
(2) Prep QC Balch: MP8694
RL = Reporting Limit
MDL = Method Detection Limit
MDL
1.2
0.20
1.1
Units DF
ug/1 I
ug/1 I
ug/1 I
Prep Analyzed By Method Prep Method
10/04/05 10/05/05 DM SW846 60108 I SW846 3010A 2
10/04/05 10/05105 DM SW846 60l0B I SW846 3010A 2
10/04105 10/05105 DM SW846 60108 I SW846 3010A 2
U = lndicales a result < MDL
B = Indicates a result > = MDL but < RL
11!111!'1 1 5 of 2 2
l;i ACX:::U I ES I.
FJSJ40
• •
Accutest Laboratories
Report of Analysis Page I or I II
Client Sample ID: WW-33
Lab Sample ID: F35340-7
Matrix: AQ -Ground Water
Method: SW846 8260B
Project: GELS; East Flat Rock, NC
Run #I
Run #2
\Run #I
Run #2
CAS No.
71-43-2
67-66-3
107-06-2
156-59-2
156-60-5
127-18-4
79-01-6
75-01-4
CAS No.
1868-53-7
17060-07-0
2037-26-5
460-00-4
File ID
M0007895.D
Purge Volume
5.0 ml
Compound
Benzene
Chloroform
DF
I
1,2-Dichloroethane
cis-1, 2-Dichloroethylene
trans-1,2-Dichloroethylene
Tetrachloroethylene
Trichloroethylene
Vinyl chloride
Surrogate Recoveries
Dibromofluoromethane
1,2-Dichloroethane-D4
Toluene-D8
4~Bromonuorobenzene
Analyzed
10/12/05
Result
ND
ND
ND
ND
ND
ND
ND
ND
Run# I
98%
97%
103%
IOI%
Date Sampled: 09/28/05
Date Received: 09/30/05
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
KK n/a n/a VM338
RL MDL Units Q
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
1.0 0.50 ug/1
Run# 2 Limits
86-115%
73-126%
86-112%
83-119%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates anaiyte found in associated method blank
N = Indicates presumptive evidence or a compound
111!'.1 16 of 22
;iACCUIESI.
F353,I0
•
Accutest Laboratories
Client Sample ID:
Lab Sample ID:
Matrix:
WW-33
F35340-7
AQ -Ground Water
Report of Analysis
Date Sampled: 09/28/05
Date Received: 09/30/05
Percent Solids: n/a
Page I of I IZ
Project: GELS; East Flat Rock, NC
Metals Analysis
Analyte Result RL
Lead 11.2 5.0
Manganese 0.74 B 15
Nickel I.I u 40
(I) Instrument QC Batch: MA4600
(2) Prep QC Batch: MP8694
RL = Reporting Limit
MDL = Method Detection Limit
MDL
1.2
0.20
I.I
Units OF
ug/1
ug/1
ug/1
Prep Analyzed By Method Prep Method
10/04/05 10/05/05 DM SW846 6010B I SW846 3010A 2
10/04/05 10/05/05 DM SW846 6010B I SW846 3010A 2
10/04/05 10/05/05 DM SW846 60108 I SW846 3010A 2
U = Indicates a result < MDL
B = Indicates a result > = MDL but < RL
111!1 17 of 22
gACCU,ESi.
F35J40
www.geotransinc.com
Dr. Gary Hill
250 Old TyTy Road
Tifton, GA 31794-6607
Reference:
Dear Dr. Hill:
Groundwater Sampling Results
September 2004
GeoTrans Project No. 2204.076.01
Oo80 Holcomb Bridge Road
Building 100, Suite 190
Roswell, GA 30076
770-642-1000 FAX [phone]
February 14, 2005
Per your request, the results from the recovery and monitoring wells on your property are
provided. The groundwater was analyzed for seven target volatile organic compounds (VOCs), one semi-
volatile organic compound (SVOC), and five metals. All field and laboratory methods utilized were
approved by the U.S. Environmental Protection Agency (EPA). The results from September 2004 for MW-
64, MW-64A, MW-66 and RWSF-l(see Figure I) are provided in the attached laboratory reports and are
summarized in the attached tables.
EPA requires General Electric to sample the wells semi-annually as part of a long-term monitoring
plan. The groundwater will be sampled for seven VOCs, and five metals. Measurements take place in the
months of March and September. The one SVOC, nitrobenzene, will be sampled only during the annual
sampling events that occur in September of every year. In the event that nitrobenzene is recovered during
the annual sampling event it will be placed back onto the list for semi-annual sampling.
We will continue to report groundwater sampling results to you as they become available. If you
have any questions, please feel free to call me at [phone] or Mr. Barry Hallock at [phone].
cc. Michael Townsend (EPA)
Barry Hallock (GELS)
David Mattison (NCDENR)
P:\GE\DOCS\Resident\Hil!Results\Hill Results 12-04.doc
Sincerely,
Project Scientist
Explanation
• Site monitor well
♦ Recovery well + Sampled Residential well
(::-: Piezometer 0
------IRWSF-2 ♦ ~ .....
RWSF-3
RWSF~
--
LOCATION:
300 600
SCALE IN FEET
•
~ -N-
I
•
FIGURE:
1
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results.
Parameter
voes (µg/LJ
1,2-Dichloroethane
Benzene
Remediation MW-64
Goal Sep-00 Dec-00 Mar-01 Jun-01
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (IO) ND (IO) ND (1.0) ND (IO)
1.0 J ND (2.0) ND (2 0) ND (2.0) ---------·------------
Sep-01 Dec-01 Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (IO) ND (IO) ND (IO) ND (1.0) ND(l.0)
. -----·-----------------·--
ND (2.0) ND (2.0) ND(2.0) ND (2.0) ND (2 0) ND (2.0) Chloroform
cis-1,2-Dichloroethene
Tetrachloroethene
trans-1,2-Dichloroethene
Trichloroethene
·----------------------·---·---· -----------------------
70 ND (2.0)
3.6
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ----------
2.8 0.83 J 1.9 J 5.0
ND (2.0)
ND (2.0)
3.0
ND (2.0) ND (2.0) ND (2.0)
1.2 J 4.0
ND (2.0) ND (2.0)
ND (2.0)
ND (2.0)
ND (2.0) 70
2.8
ND (2.0J
ND (2.0)
ND (I.OJ
ND (2.0J
ND (2.0)
ND(l.0)
ND(2.0)
ND (2.0)
ND(I.O)
ND (2.0)
ND (2.0)
ND (IO)
ND (2.0)
ND (2.0)
ND (1.0)
0.54]
ND (2.0J
ND (2.0)
ND(I.0)
-------
Vinyl chloride
SVOCs (µg/L)
Nitrobenz.ene ND (5.0)
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
2000 37.9 B ----------------------
4
15
ND (5.0)
ND(2.0)
ND (1.0)
ND (5.5)
53.0J 20.1 J
0.68 U 0.51 U
ND (5.0) ND (5.0)
22.0J 37.9 J
0.75 U 0.67 U ----------------------
3.4 U
2.7 UJ
uu
2.7 U
1.2 U
3.4 UJ
ND (5.0)
34.5 J
0.45 J
4.7 U
7.0 J
NA
36.8}
0.22 U
16.3 J
ND (2.0) ND (2.0)
ND (1.0) ND (IO)
NA ND (5.0)
25.6] 55.5 J
0.26 U 0.26U
4.7 J 16.7 Manganese
Nickel
50
100
0.68 J
1.5 J
8.4 I
5.4 U
12.7
27.7
0.8U
--------------------------------------·-·
1.2 J 0.8 U 0.8U 0.8 V I.SJ I.IV 1.1 u ---- ------------·---------------------------·-------------------------------------------·-. ----
Notes: ----------------------------------·---------------------·--------------··-· ------
U,ND -not detected
J -detected, estimated result
UJ -not detectad, estimated result
D -dilution sample
E · exceed calibration llmtt
9 -found In blank
NA -not analyzed
Bolded values indicate detected concentrations greater than remediation goals. ---------------------
ND (2.0)
ND (1.0)
NA
16.8 J
0.26 U
6.4 J
I.IV
•
Table 1. Shepherd Fann Subsite -Performance Well Analytical Results.
Parameter
voe, (µg/L)
Remediation
Goal Mar-03
MW-64
Jun-03 Sep-03 Mar-04
--------------
1,2-Dichloroethane
Benzene
Chloroform
cis-1,2-Dichloroethene
Tetrachloroethenc
trans-1,2-Dichloroethene
70
ND (2.0J
ND(l.OJ
ND (2.0J
ND(2.0J
ND (2.0J ND (2 0)
ND (I.OJ ND (1.0)
ND (2.0J ND(2.0J
ND (2.0J ND (2.0J ------·--------------·-···------·---
ND (2.0) ND (2.0) ND (2.0J
70 ND (2.0J ND (2.0J ND(2.0)
ND(2.0J
ND (I.OJ
ND (2.0J
ND (2.0J
ND (2.0)
ND (2.0)
-·------------------. ---------------------------------
Trichloroethene 2.8 ND (2.0) ND (2.0) ND (2.0)
------------------·--------·---·--------------
Vinyl chloride ND(l.OJ
SVOCs (µg/L)
Nitrobenzene JO NA
METALS TOTAL (µg/L)
Barium
Beryllium
2000 15.2 J
4 1.4J
Lead 15 4.7 U ·-----------------------
Manganese
Nickel
50
100
3.4]
ND (I.OJ ND(l.OJ
ND (5.0)
--------· ----
18.9 J 61.0J
0.26 U 0.26 U
1.2 U 15.7
1.6 J 36.8
LIU I LO J -·-------
ND (2.0)
ND (1.0)
23.21
0.3 U
4.3 J
8.0 J
LI J
Sep-04 Mar-05 Sep-05 Mar-06
-------·------
ND (2.0J
ND(l.OJ
ND (2.0) ----------
ND (2.0J
ND(2.0)
ND (2.0)
ND (2.0)
ND (I.OJ
ND(5.I)
97.5 B
0.8 U
12.1
37.6 U
5.8 B
------------Notes: -
U,NO-notdetacbtd Bolded vaJues indicate detected concentrations greater than remediation goals.
J • detected, estimated mutt
UJ -not detected, estimated result
D • dilution sampte
E -exceed calibration limit
B •found In blank
NA • not analyzed
Sep-06 Mar-07
•
• •
Accutest LabLink@31882 11: 17 21-Jan-2005
Report of Analysis Page I of 1
Client Sample ID: MW-64
Lab Sample ID: F26768-16 Date Sampled: 09/14/04
Matrix: AQ -Ground Waler Date Received: 09/16/04
Method: SW846 8270C SW846 3510C Percent Solids: n/a
Project: GELS: East Flat Rock, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F006776.D 1 10/01/04 ME 09/21/04 OPl1351 SF404
Run #2
Initial Volume Final Volume
Run #1 980 ml 1.0 ml
Run #2
CAS No_ Compound Result RL MDL Units Q
98-95-3 Nitrobenzene ND 5.1 1.0 ug/1
CAS No. Surrogate Recoveries Run# I Run# 2 Limits
367-12-4 2-Fluorophenol 50% 19-90%
4165-62-2 Phenol-d5 32% 10-68%
118-79-6 2, 4, 6-Trlbromophenol 85% 36-137%
4165-60-0 Nltrobenzene-d5 72% 49-119%
321-60-8 2-Fluorobiphenyl 77% 45-118%
1718-51-0 Terphenyl-dl 4 85% 46-135%
ND = Nol detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence .of a compound
mll!I 52. gAcon
F26768
• • Accutest LabLink@31882 11:17 21-Jan-2005
Report of Analysis Page I of 1
Client Sample IO:
Lab Sample IO:
Matrix:
Method:
MW-64
F26768-16
AQ -Ground Water
SW846 8260B
Project: GELS; East Flat Rock. NC
File IO OF Analyzed By
Run #1 N0000778.D 1 09/24/04 NJ
Run #2
IRun #I
Purge Volume
5.0 ml
Run #2
CAS No. Compound Result RL
71-43-2 Benzene ND 1.0
67-66-3 Chloroform ND 2.0
107-06-2 I , 2-Dichloroethane ND 2.0
156-59-2 cls-1,2-Dichloroethylene ND 2.0
156-60-5 trans-1,2-Dichloroethylene ND 2.0
127-18-4 Tetrachloroethylene ND 2.0
79-01-6 Trichloroethylene ND 2.0
75-01-4 Vinyl chloride ND 1.0
Date Sampled: 09/14/04
Date Received: 09/16/04
Percent Solids: n/a
Prep Date Prep Batch Analytical Batch
n/a n/a VN37
MDL Units Q
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
CASNo. Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 10196
17060-07-0 I, 2-Dichloroethane-D4 10596
2037-26-5 Toluene-DB 101%
460-00-4 4-Bromofluorobenzene 102%
ND = Not detected MDL -Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range
86-115%
73-126%
86-112%
83-119%
d,?< \ v
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
1111!1 51
11:iACCU"T
F26768
•
Accutest LabLink@31882 II :17 21-Jan-2005
Cllent Sample ID:
Lab Sample ID:
Matrix:
MW-64
F26768-16
AQ -Ground Water
Report of Analysis
Date Sampled: 09/14/04
Date Received: 09/16/04
Percent Solids: n/a
Page I of I
Project: GELS; East Flat Rock, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Barium 97.5 B 200 I.I ug/1 1 09/29/04 10/04/04 DM SW846 6010B 1 SW846 3010A 2
Beryllium 0.80 U 4.0 0.80 ug/1 1 09/29/04 10/04/04 DM SW846 6010B I SW846 3010A 2
Lead 12.1 5.0 2.9 ug/1 1 09/29/04 10/04/04 DM SW846 6010B I SW846 3010A 2
Manganese 37.6 l).. 15 0.60 ug/1 I 09/29/04 10/04/04 DM SW846 6010B I SW846 30 I 0A 2
Nickel 5.8 B 40 0.80 ug/1 I 09/29/04 10/04/04 DM SW846 6010B I SW846 3010A 2
(I) Instrument QC Batch: MA4008
(2) Prep QC Batch: MP7186
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit B = Indicates a result > = MDL but < RL
12aJ
F26768
Table 1. Shepherd Fann Subsite -Perfonnance Well Analytical Results. (continued)
Remediation MW-64A
Parameter Goal Sep-00 Dec-00 Mar-01 Jun-OJ Sep-01 Dec-01
voes (µg/L)
------
I ,2-Dichloroethane ND (20) ND (2.0) ND (2.0) ND(20) ND (2.0) ND (2.0) -------------------
Benzene ND(l.O) ND (1.0) ND (1.0) ND (1.0) ND (LO) ND (1.0) ------------
Chloroform ND (2.0) ND (2.0) ND (2.0) 0.681 0.68 J ND (2.0) ---------------· ·------------------------
cis-l ,2-Dichloroethene 70 ND (2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0)
Tetrachloroethene 50.2 46.7 43.1 41.8 42.8 41.8
.. -----------------------------·-------·
trans-1,2-Dichloroethene 70 ND (2 0) ND (2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0)
Trichloroethene 2.8 ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) -------------------------
Vinyl chloride ND (1.0) ND (1.0) ND(l.O) ND (1.0) ND (1.0) ND (1.0) -·---------··-----. --------·-·-----
SVOCs (µg/L)
Nitrobenz.ene IO ND (5.0) ND (5.0) ND(5.0) ND (5.0) ND (5.0) ND (5.0) ---------··-·
METALS TOTAL (µg/L)
Barium 2000 34.0J 33.6 J 36.0 J 32.71 29.7 J 30.21
Beryllium 4 0.79 U 0.86 VJ 0.76 U 0.83 U 0.6U 0.22 U
Lead 15 1.2 U 1.7 VJ 2.5 U 1.4 U 1.2 J 4.4 U
Manganese 50 90.7 76.9J 92.4J 70.8 Sl.4J S0.4
Nickel 100 l.9U 0.8 VJ 0.97 J 0.8 U 0.8U 0.8 U -----------------------------------·----
Notn: · --·-------B~Jd~-val-u-;-indicate detected concentrations greater than remediation goals.
U,ND -not det8Cted
J • detected, estimated result
UJ • not detected, estimated result
D-dilution sample
E -exceed calibration limit
B -found In blank
NA -not anaty.r:ttd
Mar-02 Jun-02 Sep-02 Dec-02
ND(2.0) ND (2.0) ND (2.0) ND (2.0)
------------------
ND (1.0) ND(l.O) ND (1.0) ND (1.0) • ---------·-· -------
0.77 J 0.75 J 0.741 0.8 J
ND (2.0) ND (2.0) ND(2.0) ND (2.0)
43.8 37.2 36.3 29.5 -------------------------
ND (20) ND (2.0) ND (2.0) ND (2.0)
ND{2.0) ND (2.0) ND (2.0) ND (2.0)
ND(l.0) ND (1.0) ND (1.0) ND (1.0)
·-----
NA NA ND (5.0) NA
--------------
3 l.8 J 32.1 J 32.4 J 42.8 J • 0.22 U 0.26 U 0.26 U 0.26 U
2.7 J l.2 U 1.8 U uu
54.0J 93.4 99.5 216 ----
0.8 U I.I u I.I u 1.1 u ----------
Table 1. Shepherd Fann Subsite -Perfonnance Well Analytical Results. (continued)
Parameter
voes (µg/L)
Remediation
Goal Mar-03 Jun-03
MW-64A
Sep-03 Mar-04 Sep-04 Mar-05 Sep-05 Mar-06 Sep-06 Mar-07
----------------------------------------------------------------------------
1,2-Dichloroethane ND (2.0) ND (2.0)
Benzene ND (1.0) ND (1.0) ----
Chloroform 0.65 J 0.63 J
cis-l ,2-Dichloroethene 70 ND (2.0) ND (2.0)
ND (2.0)
ND (1.0)
0.51 J
ND (2.0)
ND (2.0)
ND (1.0)
0.661
ND(2.0)
ND(2.0)
ND (1.0)
0.65 J
ND (2.0)
-------------------------------------------------------------------
Tetra.chloroethene 34.9 33.7
trans-1,2-Dichloroethene 70 ND (2.0) ND (2.0)
------
Trichloroethene ND (2.0) ND (2.0)
Vinyl chloride ND (1.0) ND (1.0)
SVOCs (µg/L)
38.0 40.9 41.7
------------------------
ND (20) ND (2.0) ND (2.0)
------·--------------------------
ND (2.0)
ND(l.0)
ND(2-0)
ND (1.0)
ND (2.0) --------------------
ND (1.0)
--·---------------·-· -----------------------------------------
N itrobenz.ene 10 NA ND (5 0) ND (5.0) ----------
METALS TOTAL (µg/L)
----------------------------------
Barium 2000 35_7 J 36,8 J 37.4] 35.6 J 33.4 B
Beryllium 4 0.26 U 0.26U 0.26 U 0.3 U O.JU
Lead 15 1.3 U 1.2 u 1.2U 1.2 J 1.2U
Manganese 50 137 264 167 126 8Ui
-··-----
Nickel 100 II U 1.1 u 1.1 u 1.1 u 1.1 u ----------------------------
---------Notes:
U,ND -not detected
Bolded values indicate detected concentrations greater than remediation goals.
J • detected, estimated result
W • not detected, estimated r9SUlt
D -dilution sample
E -exceed callbratlon limit
B -found In blank
NA • not analyzed
•
•
Accutest LabLink@31882 11:17 21-Jan-2005
Client Sample ID:
Lab Sample ID:
Matrix:
MW-64A
F26768-l 7
AQ -Ground Water
Report of Analysis
Date Sampled: 09/14/04
Date Received: 09/16/04
Percent Solids: n/a
Page 1 of 1
Project: GELS; East Flat Rock, NC
Metals Analysis
Analyte Result RL
Barium 33.4 B 200
Beryllium 0.80 U 4.0
Lead 2.9 U 5.0
Manganese 81.5 15
Nickel 0.80 U 40
(1) Instrument QC Batch: MA4008
(2) Prep QC Batch: MP7186
RL = Reporting Limit
MDL = Method Detection Limit
MDL
1.1
0.80
2.9
0.60
0.80
Units DF Prep Analyzed By Method Prep Method
ug/1 1 09/29/04 10/04/04 OM SW846 60 !OB l SW846 3010A 2
ug/1 1 09/29/04 10/04/04 OM SW846 60108 l SW846 3010A 2
ug/1 1 09/29/04 10/04/04 OM SW846 60I08 1 SW846 3010A 2
ug/1 09/29/04 10/04/04 OM SW846 60108 1 SW846 3010A 2
ugn 09/29/04 10/04/04 OM SW846 60I08 l SW846 3010A 2
U = Indicates a result < MDL
B = Indicates a result > = MDL but < RL
lb~
F26768
•
Accutest LabLink@31882 11:17 21-Jan-2005
Report of Analysis Page 1 of I
Client Sample ID: MW-64A
Lab Sample ID: F26768-17 Date Sampled: 09/14/04
Matrix: AQ -Ground Waler Date Received: 09/16/04
Method: SW846 8260B Percent Solids: n/a
Project: GELS; East Flat Rock, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #I N0000779.D I 09/24/04 NJ n/a n/a VN37
Run #2
!Run #1
Purge Volume
5.0 ml
Run #2
CASNo. Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 0.50 ug/1
67-66-3 Chlorofonn 0.65 2.0 0.50 ug/1 J 107-06-2 I, 2-Dlchloroelhane ND 2.0 0.50 ug/1
156-59-2 cls-1,2-Dlchloroethylene ND 2.0 0.50 ug/1
156-60-5 trans-I , 2-Dichloroelhylene ND 2.0 0.50 ug/1
127-18-4 Telrachloroethylene 41.7 2.0 0.50 ug/1
79-01-6 Trichloroelhylene ND 2.0 0.50 ug/1
75-01-4 Vinyl chloride ND 1.0 0.50 ug/1
CASNo. Surrogate Recoveries Run# I Run# 2 Limits
1868-53-7 Dibromofluoromethane 101% 86-115%
17060-07-0 I, 2-Dichloroethane-D4 105% 73-126%
2037-26-5 Toluene-D8 100% 86-112%
460-00-4 4-Bromofluorobenzene 100% 83-119%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
• •
Accutest LabLink@31882 II: 17 21-Jan-2005
Report of Analysis Page I of I
Client Sample ID: MW-64A
Lab Sample ID: F26768-17 Date Sampled: 09/14/04
Matrix: AQ ~ Ground Water Date Received: 09/16/04
Method: SW846 8270C SW846 3510C Percent Solids: n/a
Project: GELS; East Flat Rock, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #I F006777.D I 10/01/04 ME 09/21/04 OPll351 SF404
Run #2
Initial Volume Final Volume
Run #I 1000ml 1.0 ml
Run #2
CAS No. Compound Result RL MDL Units Q
98-95-3 Nitrobenzene ND 5.0 1.0 ug/1
CAS No. Surrogate Recoveries Run# I Run# 2 Limits
367-12-4 2-Fluorophenoi 54% 19-90%
4165-62-2 Phenol-d5 34% 10-68%
118-79-6 2, 4, 6-Tribromophenol 84% 36-137%
4165-60-0 Nitrobenzene-d5 81% 49-119%
321-60-8 2-Fluorobiphenyl 82% 45-118%
1718-51-0 Terphenyl-dl 4 85% 46-135%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
12cc:Jf
F26768
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Parameter
voe, (µg/L)
1,2-Dichloroethane
Remediation
Goal
------------
Sep-00
ND (2.0)
MW-66
Dec-00 Mar-01 Jun-01 Sep-01
---------..
ND (2.0) ND(2.0) ND (2.0) ND (2.0)
Dec-01
ND (2.0)
·------··-·------------------. ---·· ------------------·---
Benz.ene ND (1.0) ND (1.0) ND (1.0) ND (J.0) ND (1.0) ND (1.0)
----·-----·-
Chloroform ND (2.0) ND (2.0) 0.81 J ND (2.0) 0.77 J ND (2.0)
·----------------------------------------------------------
cis-1,2-Dichloroethene 70 1.6 J ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
----·--·-------------·-
T etrachloroethene 23.2 J 45.8 SJ.4 S4.S 6S.7 58.S
----------
trans-1,2-Dichloroethene 70 ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
--·---------------------------
Trichloroethene 2.8 0.94 J ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) --------------
Vinyl chloride ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND(I.O) --------
SVOCs (µg/L)
-----·-·----------------------
N itrobenzene 10 ND (5.0) ND (5.0) ND (5.5) ND (5.0) ND (5.0) ND (5.0)
------------
METALS TOTAL (µg/L)
--·-------------···--·-.
Barium 2000 52.3 J 36.1 J 39.6 J 26.0J 40.0 J 39.2 J
-------------
Beryllium 4 1.5 U 0.87 UJ 0.8U 0.94 U 0.81 U 0.22 U
Lead 15 4.2 J 1.6 UJ 3.8 U 1.6 U 1.9 J 6.3U ---
Manganese 50 223 S7.3J 81.2 20.4 119.o·J 98.9 ----------
Nickel 100 5.3 U 1.8 J !.SU 0.8 U 1.2 J 1.9 J
Notes: ---------------Ei~idecT;~~~-~di~t~~ted concentrations greater than remediation goals.
U,ND -not detected
J -detected, estimated result
UJ -not detact:od, estimated result
D -dllutlon sample
E -exceed callbratlon llznlt
B -found In blank
NA -not analyzed
Mar-02 Jun-02 Sep-02 Dec-02
-----------·
ND (2.0) ND (2.0) ND (20) ND (2.0)
------------------
ND (1.0) ND (J.0) ND (1.0) ND (1.0)
-------------·---------• 0.85 J 0.65 J 0.69 J 0.7 J --------------
ND (2.0) 0.52 J 0.55 J ND (20)
61.1 64.8 71.3 76.6
-----------
ND (2.0) ND (2.0) ND (2.0) ND (20) ---------
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
-----------
ND (1.0) ND (I.OJ ND (1.0) ND (1.0)
NA NA ND (5.0) NA ------------------
-----------------------·----------
28.0 J 26.5 J 30.8 J 28.9 J • 0.22 U 0.26 U 0.26U 0.26 U ----··------------·-·--
2.5 J 1.2 U 2.5 U 1.2 U -·---------------
16.4 J 25.9 45_0 38.8
------·-·
0.8U I.I u I.I u I.I u
Table 1. Shepherd Fann Subsite -Perfonnance Well Analytical Results. (continued)
Remediation MW-66
Parameter Goal Mar-03 Jun-03 Sep-03 Mar-04 Sep-04 Mar-OS Sep-OS Mar-06 Sep-06 Mar-07
voes (µg/L)
------------------------------
1,2-Dichloroethane
Benzene
Chloroform
cis-1,2-Dichloroethene 70
ND(2.0)
ND(LO)
0.661
0.891
ND (2.0)
ND (1.0)
0.59 J
0.19}
ND (2.0)
ND (1.0)
0.691
0.97 J
ND (2.0)
ND (1.0)
ND (2.0)
0.81 J
ND (2.0)
ND (LO)
ND(2.0)
I.OJ
-----------------------
---------------------------------------------·------------------
Tetrachlorocthene 80.2 83.0 76.6 80.4 82.1 -------·------
trans-1,2-Dichloroethene 70 ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
-----------------------------------
Trichloroethene
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene
2.8
10
METALS TOTAL (µg/L)
Barium 2000
------·---
Beryllium 4 -·---·-
Lead 15
-------·---------
Manganese 50
Nickel 100
-------
Notes:·-.. ----. ---. ----· ----
U,ND -not detec:ted
J -detected, ntfmlltltd result
UJ • not det9cted, estimated mutt
D -dilution umple
E -exceed callbratlon llmlt
B -found In blank
NA • not anatyzed
ND (2.0) ND (2.0) ND (2 0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (LO) ND (1.0) ND (LO)
NA ND (5.0) ND (5.0) -------------------------------·------
----------------------------. ---·--
22.5 1 22.8 J 22.7 J 24.61 23.6 B
0.26 U 0.26U 0.26 U 0.3 U 0.8 U
1.4 U 1.2U 1.2U L3 J 2.9U
6.6 J 14.1 J 5.9 J 4.5 J 15.9U
I.I u I.I u I.I u I.I u 0.8 U
Balded values indicate detected concentrations greater than remediation goals.
•
•
•
Accutesl LabLink@31882 11:17 21-Jan-2005
Client Sample ID:
Lab Sample ID:
Matrix:
MW-66
F26768-15
AQ -Ground Water
•
Report of Analysis
Date Sampled: 09/14/04
Date Received: 09/16/04
Percent Solids: n/a
Page I of I
Project: GELS; East Flat Rock, NC
Metals ,Analysis
Analyte Result RL
Barium 23.6 B 200
Beryllium 0.80 U 4.0
Lead 2.9 U 5.0
Manganese 15.9 I,(. 15
Nickel 0.80 U 40
(I) Instrument QC Batch: MA4008
(2) Prep QC Balch: MP7186
· RL = Reporting Limit
MDL = Method Detection Limit
MDL
I.I
0.80
2.9
0.60
0.80
Units DF Prep Analyzed By Method Prep Method ·
ugn 09/29/04 10/04/04 DM SW846 6010B I SW846 3010A 2
ugn 09/29/04 10/04/04 DM SW846 60108 I SW846 3010A 2
ugn 09/29/04 10/04/04 DM SW846 6010B I SW846 3010A 2
ugn 09/29/04 10/04/04 DM SW846 6010B l SW846 3010A 2
ugn 09/29/04 10/04/04 DM SW846 6010B 1 SW846 3010A 2
U = Indicates a result < MDL
B = Indicates a result > = MDL but < RL
F26768
• •
Accutest LabLink@31882 11:17 21-Jan-2005
Report of Analysis Page I of I
Client Sample JD: MW-66
Lab Sample ID: F26768-15 Date Sampled: 09/14/04
Matrix: AQ -Ground Water Date Received: 09/16/04
Method: SW846 8260B Percent Solids: n/a
Project: GELS; East Flat Rock, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #I N0000777.D I 09/24/04 NJ n/a n/a VN37
Run #2
\Run #I
Purge Volume
5.0 ml
Run #2
CASNo. Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 0.50 ug/l
67-66-3 Chloroform ND 2.0 0.50 ug/l
l07-06-2 1,2-Dichloroethane ND 2.0 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene 1.0 2.0 0.50 ug/l 1
156-60-5 trans-1,2-Dichloroethylene ND 2.0 0.50 ug/l
127-18-4 Tetrachloroethylene 82.1 2.0 0.50 ug/l
79-01-6 Trichloroethylene ND 2.0 0.50 ug/1
75-01-4 Vinyl chloride ND 1.0 0.50 ug/1
CASNo. Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane l00% 86-115%
17060-07-0 I, 2-Dichioroethane-D4 107% 73-126%
2037-26-5 Toluene-DH IOI% 86-112%
460-00-4 4-Bromofluorobenzene l02% 83-119%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates anaiyte found in associated method blank
N = Indicates presumptive evidence of a compound
•
Accutest LabLink@31882 11:17 21-Jan-2005
Report of Analysis Page I of I
Client Sample ID: MW-66
Lab Sample ID: F26768-15
Matrix: AQ -Ground Water
Method: SW846 8270C SW846 3510C
Project: GELS: East Flat Rock, NC
File ID DF Analyzed
Run #I F006775.D I 09/30/04
Run #2
Initial Volume Final Volume
Run #I 1000ml 1.0 ml
Run #2
CAS No. Compound Result
98-95-3 N ilrobenzene ND
CAS No. Surrogate Recoveries Run# I
367-12-4 2-Fluorophenol 57%
4165-62-2 Phenol-d5 36%
118-79-6 2,4,6-Tribromophenol 85%
4165-60-0 Nitrobenzene-d5 84%
321-60-8 2-Fluorobiphenyl 83%
1718-51-0 Terphenyl-d14 85%
Date Sampled:
Date Received:
Percent Solids:
By Prep Date
ME 09/21/04
RL MDL Units
5.0 1.0 ug/1
Run# 2 Limits
19-90%
10-68%
36-137%
49-119%
45-118%
46-135%
09/14/04
09/16/04
n/a
Prep Batch
OPll351
Q
Analytical Batch
SF404
A ✓( r:~r?
v
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
1W
f26768
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Parameter
voes (µg/L)
Remediation
Goal Sep-00 Dec-00
RWSF-1
Mar-01 Jun-01 Sep-01 De<-01 Mar-02 Jun-02 Sep-02
----------··--------------·----··--·---------------------------
1,2-Dichloroethane ND (2.0) ND (2.0) ND (2.0) ND (2.0) --------------------------------
Benzene ND (J.0) ND (1.0) ND(I.O) ND(J.O)
---
Chloroform ND(2.0) ND (2.0) ND (2.0) ND(2.0)
cis-1,2-Dichloroethene 70 ND (2.0) ND (2.0) ND (2.0) ND (2.0) -------------------
Tetrachloroethene 34.0 !§1.4 43.2 40.4
trans-1,2-Dichloroethene 70 ND (2.0) ND (2.0) ND (20) ND (2.0)
ND (2.0)
ND(J.0)
ND(2.0)
ND (2.0)
46.J
ND (2.0)
ND (2.0)
ND (1.0)
ND (2.0)
ND (2.0)
52.6
ND (2.0)
ND (20)
ND (1.0)
ND(20) ND(20)
ND (1.0) ND (1.0)
0.52 J ND (2.0) 0.52 J
ND (2.0) ND (2.0) ND (2.0)
56.J 56.4 43.2
ND (2.0) ND (2.0) ND (2 0)
Dec-02
ND (2.0)
ND (1.0)
ND (2.0)
ND (2.0)
63.6
ND (2.0) ------------~ ·---~---·-------------------
Trichloroethene 2.8 ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND~ ND~ ND~~ ND~ ND~ -------------··-----·-----------
Vinyl chloride ND(l.0) ND (1.0) ND(l.O) ND(l.O) ND(l.O) ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0)
SVOCs (µg/L)
Nitrobenzene ND (5.0) ND (5.0) ND (5.5) ND (5.5) ND (5.0) ND (5.0) NA NA ND (5.0) NA
METALS TOTAL (µg/L)
Barium 2000 161.0 J 193.0 J 290 242.0 254.0 J 153,0 J 156.0J 142.0J 134.0J 61.3 J ----
Beryllium 4 0.3U 2.6UJ 2.2U 2.3 U I.I J 1.21 0.22 U 0.26 U 0.26 U 0.26 U ---------
Lead 15 1.5 J S0.6J 49.5 21.4 24.J 10.4 U 26.1 22.7 18.4 l.2U --------------------·----~------------------·--------------
Manganese 50 65.6 42.6 J 109,0 J 100.0 90.1 J 71.8 J 98.I J !OS 77.6 0.16U
Nickel 100 13.7 J 1.4 J 6.5 J 0.8 U 3.5 J 1.8 J 4.2 J I.I u I.I u I.I u
----------------
N~: ----
U,NO • not detected
J • detected, nttmal:9<1 result
UJ -not detected, estimated mutt
D -dlluUon sample
E • exceed calibration lbnlt
B -found In blank
NA -not analyzed
-------------------· -----·-----------·-----------
Bolded values indicate detected concentrations greater than remediation goals.
•
•
Table 1. Shepherd Fann Subsite -Perfonnance Well Analytical Results. (continued)
Parameter
voes (µg/L)
1,2-Dichloroethane
Remediation
Goal Mar-03
ND (2.0)
RWSF-1
Jun-03 Sep-03 Mar-04 Sep-04
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
Mar-05 Sep-05 Mar-06 Sep-06
----------·---------------------
Benzene ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0) -------··---------------------------------
Chloroform ND (2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0) ---·-----------------· -------
cis-1,2-Dichloroethene 70
-----··-----
Tetrachloroethene
·-·--··
trans-1,2-Dichloroethene 70
Trichloroethene 2.8
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene 10
METALS TOTAL (µg/L)
Barium 2000
Beryllium 4
--------··-···
Lead 15
Manganese 50
Nickel 100 ·---------- ----------
Notes: ----
u,No. not det9ctad
J • detected, nttmat:ed result
UJ -not detect:8d, estimated mutt
D • dllutfon sample
E -exceed callbratlon lbntt
B -found In blank
NA-notanalyud
ND (2.0) ND (2.0) 3.5 ND(2.0) ND (2.0) ------------
32.:Z 38.1 37.7 44.3 36.8
·--·-·
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND(2.0) ND (2.0) 0.91 J ND(2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (I.OJ
NA ND (5.0) ND (5.0)
28.3 J 47.61 152.0 J 141.0J 132.0 B
0.26U 0.26U 0.26 U 0.JU 0.3 U
30.5 106 7.9 14.0 13.8
12.8 J 126 64.5 55.7 106
311 100.0 1.8 J 40.8 J 10.7 B
--------------~---c----~---c--,---------------
Bolded values indicate detected concentrations greater than remediation goals.
Mar-07
•
•
Accutest LabLink@31882 11:17 21-Jan-2005
Report of Analysis Page 1 of 1
Client Sample ID: RWSE-1
Lab Sample ID: F26768-14 Date Sampled: 09/14/04
Matrix: AQ -Ground Water Date Received: 09/16/04
Method: SW846 8270C SW846 3510C Percent Solids: n/a
Project: GELS; East Flat Rock, NC
File ID OF Analyzed By Prep Date Prep Batch Analytical Batch
Run #I F006774.D I 09/30/04 ME 09/21/04 OPl1351 SF404
Run #2
Initial Volume Final Volume
Run #I 1000 ml 1.0 ml
Run #2
CAS No. Compound Result RL MDL Units Q
98-95-3 Nitrobenzene ND 5.0 1.0 ug/1
CAS No. Surrogate Recoveries Run# I Run# 2 Limits
367-12-4 2-Fluorophenol 54% 19-90%
4165-62-2 Phenol-d5 34% 10-68%
118-79-6 2, 4, 6-Tribromophenol 85% 36-137%
4165-60-0 Nitrobenzene-d5 80% 49-119%
321-60-8 2-Fluorobiphenyl 80% 45-118%
1718-51-0 Terphenyl-dl 4 83% 46-135%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
1'2~
F26766 " ·' ·
•
Accutest LabLink@31882 11:17 21-Jan-2005
Client Sample ID:
Lab Sample ID:
Matrix:
RWSE-1
F26768-14
AQ -Ground Water
Report of Analysis
Date Sampled: 09/14/04
Date Received: 09/16/04
Percent Solids: n/a
Page 1 of 1
Project: GELS; East Flat Rock, NC
Metals Analysis
Analyte Result RL
Barium 132 B 200
Beryllium 0.80 U 4.0
Lead 13.8 5.0
Manganese 106 15
Nickel 10.7 B 40
(I) Instrument QC Batch: MA4008
(2) Prep QC Batch: MP7186
RL = Reporting Limit
MDL = Method Detection Limit
MDL
I.I
0.80
2.9
0.60
0.80
Units OF Prep Analyzed By Method Prep Method
ug/i I 09/29/04 10/04/04 DM SW846 60108 I SW846 3010A 2
ug/1 I 09/29/04 10/04/04 DM SW846 60108 I SW846 30 lOA 2
ug/1 I 09/29/04 10/04/04 DM SW846 60108 I SW846 3010A 2
ug/1 09/29/04 10/04/04 DM SW846 60108 t SW846 3010A 2
ug/1 09/29/04 10/04/04 DM SW846 60108 I SW846 30 I 0A 2
U = Indicates a result < MDL
B = Indicates a result > = MDL but < RL
lb~
F26768
•
Accutest LabLink@31882 11:17 21-Jan-2005
Report of Analysis Page I of I
Client Sample ID: RWSE-1
Lab Sample ID: F26768-14 Date Sampled: 09/14/04
Matrix: AQ -Ground Water Date Received: 09/16/04
Method: SW846 8260B Percent Solids: n/a
Project: GELS; East Flat Rock, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #I N0000776.D I 09/24/04 NJ n/a n/a VN37
Run #2
\Run #I
Purge Volume
5.0 ml
Run #2
CAS No. Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 0.50 ug/1
67-66-3 Chloroform ND 2.0 0.50 ug/1
107-06-2 I, 2-Dichloroethane Nb 2.0 0.50 ug/1
156-59-2 cls-1,2-Dichloroethylene ND 2.0 0.50 ug/1
156-60-5 trans-I, 2-Dichloroethylene ND 2.0 0.50 ug/1
127-18-4 Tetrachloroethylene 36.8 2.0 0.50 ug/1
79-01-6 Trichloroethylene ND 2.0 0.50 ug/1
75-01-4 Vinyl chloride ND 1.0 0.50 ug/1
CAS No. Surrogate Recoveries Run# I Run# 2 Limits
1868-53-7 Dibromofluoromethane 102% 86-115%
17060-07-0 I, 2-Dichloroethane-D4 108% 73-126%
2037-26-5 . Toluene-DB 99% 86-112%
460-00-4 4-Bromofluorobenzene 98% 83-119%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit
E = Indicales value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
1111!1 4S ;jACCUT
F26766
www.geotransinc.co111
Dr. Gary Hill
250 Old TyTy Road
Tifton, GA 31794-6607
Reference:
Dear Dr. Hill:
Groundwater Sampling Results
March 2004
GeoTrans Project No. 2204.076.01
1080 Holcomb Bridge Road
Building 100, Suite 190
Roswell, GA 30076
770-642-1000 FAX [phone]
Per your request the results from the recovery and monitoring wells on your property are provided.
The groundwater was analyzed for seven target volatile organic compounds (YOCs) and five metals. All
field and laboratory methods utilized were approved by the U.S. Environmental Protection Agency (EPA).
The results from September 2003 for MW-64, MW-64A, MW-66 and RWSF-l(see Figure I) are provided
in the attached laboratory reports and are summarized in the attached tables.
In December 2003, EPA approved the change in monitoring frequency from quarterly to semi-
annual. Monitoring events will now take place only during the months of March and September. The one
SVOC, nitrobenzene, has been removed from the semi-annual sampling events with EPA approval. It will
be sampled only during the annual sampling events that occur in September of every year. In the event
that nitrobenzene is recovered during the annual sampling event it will be placed back onto the list for
semi-annual sampling.
We will continue to report groundwater sampling results to you as they become available. If you have any
questions, please feel free to call me at [phone] or Mr. Barry Hallock at [phone].
cc. Michael Townsend (EPA)
Barry Hallock (GELS)
David Mattison (NCDENR)
Jim Laforest (COM Federal)
P:IGEIDOCSIRESIDENDIIILL RESULTS\Hill Results3-04.doc
Sincerely,
Mtu;, ~/U((U,(/(
Patricia Hermann
Project Scientist
P.\GE\rgvplgis-rgvp\SFsite.wor
L __
--' ·----
. . ,,_ ...
l.
·~·
' .. _,' _ .. -··.,. .· .· .. ·
.
·-. I
Explanation
• Site monitor well
♦ Recovery well + Sampled Residential well
0 Piezometer
n
0
M •
RWSF-2♦
RWSF-1'-MW-,,;
-> •<:-...._ MW-6'
'•,. ',,_ MW-6,1,A '·. ----·<::.:::.---.,
'·.
300
SCALE IN FEET
600
RWSF-,.
BAPZ-7 0
TITLE:
Location of Shepherd Farm Subsite Features
LOCATION: East Flat Rock, NC
~ Geo T ~:~;:: ::; a ◄. fET~• ffCH co•mN~ Ir an S, Inc. e-,-IL-.--1--s,-,-ite ____ _J
DATE 11/30101
FIGURE·
1
•
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results.
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Benzene
Chloroform
cis-1,2-Dichloroethene 70
Tetrachloroethene
trans-1,2-Dich\oroethene 70
Trichloroethene 2.8
Vinyl chloride
SVOCs (µg/L)
Nitrobcnzene 10
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J -detected, estimated result
UJ · not detected, estimated result
D -dilution sample
E • exceed calibration limit
B -found in blank
NA • not analyzed
2000
4
15
50
100
MW-64
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0)
I.OJ ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
3.6 2.8 0.83 J 1.9 J 5.0 3.0
ND (2.0) ND (2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0)
ND (5.0) ND (5.0) ND (5.5) ND (5.0) ND (5.0) ND (5.0)
37.9 B 53.0 J 20.1 J 22.0 J 37.9 J 34.5 J
0.68 J 0.68 U 0.51 U 0.75 U 0.67 U 0.45)
1.5 J 12.7 3.4 U l.3U l.2U 4.7 U
8.4 J 27.7 2.7 UJ 2.7 U 3.4 UJ 7.0 J
5.4 U 0.8 U 1.2 J 0.8 U 0.8 U 0.8 U
Balded values indicate detected concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (I.OJ ND (1.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) • ND (2.0) ND (2.0) ND (2.0) ND (2.0)
0.54 J 1.2 J 4.0 ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0)
NA NA ND (5.0) NA
36.8 J 25.6 J 55.5 J 16.8 J • 0.22 U 0.26 U 0.26 U 0.26 U
8.8 2.8 J 7.9 1.2 U
16.3 J 4.7 J 16.7 6.4 J
1.5 J I.I u I.I u I.I U
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Benzene
Chloroform
cis-1,2-Dichloroethene
Tetrachloroethene
trans-1,2-Dichloroethene
T richloroethene
Vinyl chloride
SVOCs (µg/L)
Nitrobcnzene
METALSTOTAL(µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND • not detected
J -detected, estimated result
UJ • not detected, estimated result
D -dilution sample
E -exceed calibration limit
B -found in blank
NA -not analyzed
70
70
2.8
10
2000
4
15
50
100
MW-64
Mar-03 Jun-03 Sep-03 Mar-04 Sep-04 Mar-OS
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND {2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND {1.0)
NA ND (5.0)
15.2 J 18.9 J 61.0 J 23.2 J
1.4 J 0.26 U 0.26 U 0.3 U
4.7 U 1.2 u 15.7 4.3 J
3.4 J 1.6 J 36.8 8.0 J
l.lU I. I U I 1.0 J I.I J
Balded values indicate detected concentrations greater than remediation goals.
Sep-OS Mar-06 Sep-06 Mar-07
•
•
(
• Accutest Laboratories
Report of Analysis Page I of I
Client Sample ID: MW-64
Lab Sample ID: F22598-4
Matrix: AQ -Ground Water
Method: SW846 8260B
Project: GELS, Hendersonville, NC
Run#!
Run#2
!Run #1
Run#2
File ID
J006079.D
Purge Volume
5.0ml
DF
I
VOA TCL List
CASNo. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 1,2-Dichloroethane
156-59-2 cis-1,2-Dichloroethylene
156-60-5 trans-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CASNo. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
17060-07-0 1,2-Dichloroethane-D4
2037-26-5 Toluene-OS
460-00-4 4-Bromofluorobenzene
Analyzed
03/11/04
Result
ND
ND
ND
Nb
ND.
ND
"ND
ND
Run# 1
101%·
105%
100%
1_01 %
Date Sampled: 03/04/04
Date Received: 03/05/04
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
RA n/a n/a VJ268
RL MDL Units Q
1.0 0.50 ug/1
2.0 0.50 ug/1
2.0 0.50 ug/1
2.0 0.50 ug/1
2.0 0.50 ug/1
2.0 0.50 ug/1
2.0 0.50 ug/1
1.0 0.50 ug/1
Run#2 Limits
86-115%
73-126%
86-112%
83-119%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
008
(
• Accutest Laboratories
Client Sample ID:
Lab Sample ID:
Matrix:
MW-64
F22598-4
AQ -Ground Water
Report of Analysis
Date Sampled: 03/04/04
Date Received: 03/05/04
Percent Solids: n/a
Page I of I
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units DF Prep Analyzed By Method Prep Method
Barium 23.2'sc_ J 200 0.50 ug/1 03/15/04 03/17 /04 OM SW846 6010B I SW846 3010A 2
Beryllium 0.30U 4.0 0.30 ug/1 03/15/04 03/17/04 OM SW846 6010B 1 SW846 30 I 0A 2
Lead 4_3tr,,;..1' 5.0 1.2 ug/1 03/15/04 03/17/04 OM SW846 6010B I SW846 30 lOA 2
Manganese 8:0~ 1" 15 0.16 ug/1 03/15/04 03/17/04 OM SW846 6010B I SW846 30 lOA 2
Nickel LIB-1 40 1.1 ug/1 03/15/04 03/17/04 OM SW846 6010B I SW846 3010A 2
(I) Instrument QC Batch: MA3725
(2) Prep QC Batch: MP6457
RL = Reponing Limit U = Indicates a result < IDL
IDL = Instrument Detection Limit B = Indicates a result > = ID L but < RL
01
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Benzene
Chloroform
cis-1,2-Dichloroethene
Tetrachloroethene
trans-1,2-Dich\oroethene
Trichloroethene
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND • not detected
J -detected, estimated result
UJ · not detected, estimated result
D -dilution sample
E • exceed calibration limit
B -found in blank
NA • not analyzed
70
70
2.8
10
2000
4
15
50
l00
MW-64A
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND(l.0) ND (1.0) ND(l.0) ND (1.0)
ND (2.0) ND (2.0) ND (2.0) 0.68 J 0.68 J ND (2.0)
ND (2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
50.2 46.7 43.1 41.8 42.8 41.8
ND (2.0) ND (2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0)
ND (5.0) ND (5.0) ND (5.0) ND (5.0) ND (5.0) ND (5.0)
34.0 J 33.6 J 36.0 J 32.7 J 29.7 J 30.2 J
0.79 U 0.86 UJ 0.76 U 0.83 U 0.6 U 0.22 U
1.2 U 1.7 UJ 2.5 U l.4U 1.2 J 4.4 U
90.7 76.9 J 92.4 J 70.8 51.4J 50.4
1.9 U 0.8 UJ 0.97 J 0.8 U 0.8 U 0.8 U
Balded values indicate detected concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND(l.0)
0.77 J 0.75 J 0.74 J 0.8 J • ND(2.0) ND (2.0) ND (2.0) ND (2.0)
43.8 37.2 36.3 29.5
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0)
NA NA ND (5.0) NA
31.81 32. I J 32.4 J 42.8 J • 0.22 U 0.26 U 0.26 U 0.26 U
2.7 J 1.2 u 1.8 U 1.2 U
54.0 J 93.4 99.5 216
0.8 U I.I u I.I U 1.IU
Table 1. Shepherd Farm Subsite • Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Benzene
Chlorofonn
cis-1.2-Dichloroethene
T etrachloroethene
trans-1,2-Dichloroethenc
Trichloroethene
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene
METALS TOTAL (µg/L)
Barium
Betyllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J • detected, estimated result
UJ • not detected, estimated result
D • dilution sample
E • exceed calibration limit
B -found in blank
NA • not analyzed
70
70
2.8
10
2000
4
15
50
100
MW-64A
Mar-03 Jun-03 Sep-03 Mar-04 Sep-04 Mar-05
ND (2.0J ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND(l.0) ND (1.0)
0.65 J 0.63 J 0.51 J 0.66 J
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
34.9 33.7 38.0 40.9
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND(I.0) ND (1.0) ND (1.0) ND (1.0)
NA ND (5.0)
35.7 J 36.8 J 3 7.4 J 35.6 J
0.26 U 0.26 U 0.26 U 0.3 U
l.3U 1.2 U 1.2U 1.2 J
137 264 167 126
1.1 U I.I U 1.IU I.I U
Balded values indicate detected concentrations greater than remediation goals.
Sep-05 Mar-06 Sep-06 Mar-07
•
•
Accutest Laboratories
Report of Analysis Page I of I
Client Sample ID: MW-64A
Lab Sample ID: F22598-5
Matrix: AQ -Ground Water
Method: SW846 8260B
Project: GELS, Hendersonville, NC
Run#!
Run#2
!Run #1
Run#2
File ID
1006080.D
Purge Volume
5.0 ml
DF
1
VOA TCL List
CASNo. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 1,2-Dichloroethaoe
156-59-2 cis-1,2-Dichloroethylene
156-60-5 traos-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CASNo. Surrogate Recoveries
1868-53-7 Dibromofluoromethaoe
17060-07-0 1,2-Dichloroethaoe-D4
2037-26-5 Toluene-DB
460-00-4 4-Bromofluorobenzene
Analyzed
03/11/04
Result
.ND:
o:66 ..
ND 'No•·····
rilb
40.9.
ND
ND
Run# 1
102%
106%
99%
1.00%.
Date Sainpled: 03/04/04
Date Received: 03/05/04
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
RA n/a n/a VJ268
RL MDL Units Q
1.0 0.50 ug/1
2.0 0.50 ug/1 J
2.0 0.50 ug/1
2.0 0.50 ug/1
2.0 0.50 ug/1
2.0 0.50 ug/1
2.0 0.50 ug/1·
1.0 0.50 ug/1
Run#2 Limits
86-115%
73-126%
86-112%.
83-119%
ND = Not detected MDL -Method Detection Limit J = Indicates ao estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration raoge.
B = Indicates aoalyte found in associated method blank
N = Indicates presumptive evidence of a compound
DOE
(
• Accutest Laboratories
Client Sample Ill:
Lab Sample ID:
Matrix:
MW-64A
F22598-5
AQ -Ground Water
Report of Analysis
Date Sampled: 03/04/04
Date Received: 03/05/04
Percent Solids: n/a
Page I of I
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units DF Prep Analyzed By Method Prep Method
Barium 35,(i b-c "T 200 0.50 ug/1 I 03/15/04 03/17/04 DM SW846 60JOB I SW846 30 JOA 2
Beryllium .0.30U < 4.0 0.30 ug/1 I 03/15/04 03/17/04 DM SW846 60JOB I SW846 30 JOA 2
Lead .1.21Lt'f 5.0 1.2 ug/1 I 03/15/04 03/17/04 DM SW846 60JOB I SW846 30 JOA 2
Manganese 126 •. 15 0.16 ug/1 I 03/15/04 03/17/04 DM SW846 6010B I SW846 30 JOA 2
Nickel 1.ru·· 40 I.I ug/1 03/15/04 03/17/04 DM SW846 60 JOB I SW846 30JOA 2
(I) Instrument QC Batch: MA3725
(2) Prep QC Batch: MP6457
RL = Reporting Limit U = Indicates a result < IDL
IDL = Instrument Detection Limit B = Indicates a result > = IDL but < RL
011
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethanc
Benzene
Chlorofonn
cis-1,2-Dichlorocthene
Tetrachloroethene
trans-1.2-Dichloroelhene
Trichloroethene
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND • not detected
J -detected, estimated result
UJ -not detected, estimated result
D -dilution sample
E -exceed calibration limit
B -found In blank
NA -not analyzed
70
70
2.8
10
2000
4
15
50
100
MW-66
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND ( I.OJ ND (1.0) ND (1.0) ND (I.OJ
ND (2.0) ND (2.0) 0.81 J ND(2.0) 0,77 J ND (2.0)
1.6 J ND (2.0) ND (2.0J ND (2.0) ND (2.0) ND (2.0)
23.2 J 45.8 53.4 54.5 65.7 58.5
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
0.94 J ND (2.0) ND (2.0) ND (2.0) ND(2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (I.OJ ND (1.0)
ND (5.0) ND (5.0J ND (5.5) ND (5.0) ND (5.0) ND (5.0)
52.3 J 36.1 J 39.6 J 26.0 J 40.0 J 39.2 J
1.5 u 0.87 UJ 0.8 U 0.94 U 0.81 U 0.22 U
4.2 J 1.6 UJ 3.8 U 1.6 U 1.9 J 6.3 U
223 57.3 J 81.2 20.4 119.0J 98.9
5.3 U 1.8 J 1.8 U 0.8 U 1.2 J 1.9 J
Bolded values indica1e detected concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND (2.0) ND (2.0J ND (2.0)
ND (1.0) ND (1.0) ND (I.OJ ND (1.0)
0.85 J 0.65 J 0.69 J 0.71 • ND (2.0) 0.52 J 0.55 J ND (2.0)
6J.I 64.8 71.3 76.6
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0)
NA NA ND(5.0) NA
28.0 J 26.5 J 30.8 J 28.9 J • 0.22 U 0.26 U 0.26 U 0.26 U
2.5 J 1.2U 2.5 U 1.2U
16.4 J 25.9 45.0 38.8
0.8 U I. I U I. I U 1.IU
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Benzene
Chloroform
cis-1,2-Dichloroethene
Tetrachloroethene
trans-1,2-Dichloroethene
Trichloroethene
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J • detected, estimated result
UJ • not detected, estimated result
D • dilution sample
E -exceed calibration limit
B -found in blank
NA -not analyzed
70
70
2.8
10
2000
4
15
50
100
MW-66
Mar-03 Jun-03 Sep-03 Mar-04 Sep-04 Mar-OS
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND(l.0) ND (1.0) ND (1.0)
0.66 J 0.59 J 0.69 J ND (2.0)
0.89 J 0.79 J 0.97 J 0.81 J
80.2 83.0 76.6 80.4
ND (2.0) ND (2.0) ND(2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0)
NA ND (5.0)
22.5 J 22.8 J 22.7 J 24.6 J
0.26 U 0.26 U 0.26 U 0.3 U
l.4U 1.2 U 1.2 u I.] J
6.6 J 14.1 J 5.9 J 4.5 J
1.1 U I.JU I.I U I.I U
Balded values indicate detected concentrations greater than remediation goals.
Sep-OS Mar-06 Sep-06 Mar-07
•
•
(
• Accutest Laboratories
Report of Analysis Page I of I
Client Sample ID: MW-66
Lab Sample ID: F22598-3
Matrix: AQ -Ground Water
Method: SW846 8260B
Project: GELS, Hendersonville, NC
Run#!
Run#2
IRun #I
Run#2
File ID
J006078.D
Purge Volume
5.0 ml
DF
I
VOA TCL List
CASNo. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 1,2-Dichloroethane
156-59-2 cis-1,2-Dichloroethylene
156-60--5 trans-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CASNo. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
17060-07-0 I ,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromofluorobenzene
Analyzed
03/11/04
Result
.ND
ND
ND.
0.8( .
ND.
80.4
ND.
ND.
Run# 1
·102%
104%
99%
IOI%
Date Sampled: 03/04/04
Date Received: 03/05/04
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
RA n/a n/a VJ268
RL MDL Units Q
1.0 0.50 ug/1
2.0 0.50 ug/1
2.0 0.50 ug/1
2.0 0.50 ug/1 J
2.0 0.50 ug/1
2.0 0.50 ug/1
2.0 0.50 ug/1
1.0 0.50 ug/1
Run#2 Limits
86-115%
73-126%
86-112%
83-119%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
,I', • ~ ... ~~
\ . ' ,' . ~. .
(
• Accutest Laboratories
Client Sample ID:
Lab Sample ID:
Matrix:
MW-66
F22598-3
AQ -Ground Water
Report of Analysis
Date Sampled: 03/04/04
Date Received: 03/05/04
Percent Solids: n/a
Page 1 of 1
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units DF Prep Analyzed By Method Prep Method
Barium 24.6 'B. -s. 200 0.50 ug/1 1 03/15/04 03/17/04 DM SW846 60 JOB I SW846 30 JOA 2
Beryllium 0.30U. 4.0 0.30 ug/1 1 03/15/04 03/17/04 DM SW846 60 JOB I SW846 30 JOA 2
Lead 1.311._),' 5.0 1.2 ug/1 1 03/15/04 03/17/04 DM SW846 60 JOB I SW846 30JOA 2
Manganese 4:511,..~ 15 0.16 ug/1 1 03/15/04 03/17/04 DM SW846 60 JOB I SW846 30 JOA 2
Nickel l.l u .· 40 J.l ug/1 I 03/15/04 03/17 /04 DM SW846 60 JOB I SW846 30 I QA 2
(I) Instrument QC Batch: MA3725
(2) Prep QC Batch: MP6457
RL = Reporting Limit U = Indicates a result < IDL
IDL = Instrument Detection Limit B = Indicates a result > = IDL but < RL
01 ,, '.", JI r~ ' ,;.:_·.
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1.2-Dichloroethane
Benzene
Chlorofonn
cis-1,2-Dichloroethene
Tetrachloroethene
trans-1,2-Dichloroethene
Trichloroethene
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,NO -not detected
J -detected, estimated result
UJ • not detected, estimated result
D -dilution sample
E -exceed calibration limit
B -found in blank
NA -not analyzed
70
70
2.8
10
2000
4
15
50
100
RWSF-1
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0J ND (2.0)
ND (2.0J ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0J
34.0 51.4 43.2 40.4 46.3 52.6
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0J ND (2.0J ND (2.0)
ND (1.0) ND(I.O) ND (1.0) ND (1.0) ND (1.0) ND (1.0)
ND (5.0) ND (5.0) ND (5.5) ND (5.5) ND (5.0J ND (5.0)
161.0 J 193.0 J 290 242.0 254.0 J 153.0 J
0.3 U 2.6 UJ 2.2 U 2.3 U I.I J 1.2 J
1.5 J 50.6 J 49.5 21.4 24.3 10.4 U
65.6 42.6 J 109.0 J 100.0 90.1 J 71.8J
13.71 1.4 J 6.5 J 0.8 U 3.5 J 1.8 J
Balded values indicate detected concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (I.OJ ND (1.0) ND (1.0) ND (1.0)
0.52 J ND (2.0) 0.52 J ND (2.0) • ND (2.0) ND (2.0) ND (2.0) ND (2.0)
56.3 56.4 43.2 63.6
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0J ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (I.OJ ND (1.0)
NA NA ND (5.0) NA
156.0 J 142.0 J 134.0 J 61.3 J • 0.22 U 0.26 U 0.26 U 0.26 U
26.1 22.7 18.4 1.2 u
98.1 J 105 77.6 0.16 U
4.2 J I. I U I. I U 11 U
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Benzene
Chloroform
cis-1,2-Dichloroethene
Tetrachloroethene
trans-1,2-Dichloroethene
Trichloroethene
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J • detected, estimated result
UJ • not detected, estimated result
D • dilution sample
E • exceed calibration limit
B -found in blank
NA -not analyzed
70
70
2.8
10
2000
4
I 5
50
IOO
RWSF-1
Mar-03 Jun-03 Sep-03 Mar-04 Sep-04 Mar-OS
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND(l.0) ND (1.0) ND (1.0) ND (1.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) 3.5 ND (2.0)
32.2 38.1 37.7 44.3
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) 0.91 J ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0)
NA ND (5.0)
28.3 J 47.6 J 152.0 J 141.0 J
0.26 U 0.26 U 0.26 U 0.3 U
30.5 106 7.9 14.0
12.8 J 126 64.5 55.7
311 100.0 1.8 J 40.8 J
Balded values indicate detected concentrations greater than remediation goals.
Sep-OS Mar-06 Sep-06 Mar-07
•
•
• Accutest Laboratories
Report of Analysis Page I of I
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
RWSF-1
F22598-2
AQ -Ground Water
SW846 8260B
Project: GELS, Hendersonville, NC
Run #1
Run#2
IRun #1
Run#2
File ID
1006077.D
Purge Volume
5.0 ml
DF
I
VOA TCL List
CASNo. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 1,2-Dichloroethane
156-59-2 cis-1,2-Dichloroethylene
156-60-5 trans-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
Analyzed By
03/11/04 RA
Result RL
ND 1.0
ND. 2.0 .. ND 2.0
·ND··· 2.0
ND. 2.0
44j· ..
2.0
ND. .·. 2.0
ND 1.0
Date Sampled: 03/04/04
Date Received: 03/05/04
Percent Solids: n/a
Prep Date
n/a
MDL Units
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
Prep Batch
n/a
Q
Analytical Batch
VJ268
CASNo. Surrogate Recoveries Run# 1 Run#2 Limits
1868-53-7 Dibromolluoromethane 101%
17060-07-0 l ,2-Dichloroethane-D4 105%
2037-26-5 Toluene-DB 99%
460-00-4 4-Bromolluorobenzene 96%
ND = Not detected MDL -Method Detection Limit
RL = Reponing Limit
E = Indicates value exceeds calibration range
86-115%
73-126%
86-112%
83-119%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
,·, .. ~·· ~ J \,;,,,, >-005
• Accutest Laboratories
Client Sample ID:
Lab Sample ID:
Matrix:
RWSF-1
F22598-2
AQ -Ground Water
•
Report of Analysis
Date Sampled: 03/04/04
Date Received: 03/05/04
Percent Solids: n/a
Page I of I
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL
Barium 14111---y 200
Beryllium 0.30U 4.0
Lead 14,0 •, 5.0
Manganese 55,7 \ :-_,... 15
Nickel 40,l!,;;c · .. ) 40
(I) Instrument QC Batch: MA3725
(2) Prep QC Batch: MP6457
RL = Reporting Limit
IDL = Instrument Detection Limit
IDL
0.50
0.30
1.2
0.16
1.1
Units DF Prep Analyzed By Method Prep Method
ug/1 I 03/15/04 03/17/04 DM SW846 60 !OB l SW846 30 IOA 2
ug/1 I 03/15/04 03/17/04 DM SW846 60 !OB l SW846 3010A 2
ug/1 1 03/15/04 03/17/04 DM SW846 6010B l SW846 3010A 2
ug/1 1 03/15/04 03/17/04 DM SW846 6010B l SW846 30 IOA 2
ug/1 1 03/15/04 03/17/04 DM SW846 6010B l SW846 3010A 2
U = Indicates a result < ID L
B = Indicates a result > = IDL but < RL
016
. . t -1181.,Geo ~ '.4 'TETRATECHCOMPANY rans, Inc.
www.geotransinc.com
Dr. Gary Hill
250 Old TyTy Road
Tifton, GA 31 794-6607
Reference:
Dear Dr. Hill:
Groundwater Sampling Results
September 2003
GeoTrans Project No. 2204.028.41
• I 080 Holco111b llridg,, Road
lluilcling I 00, Suite I 'JO
Roswell, GA 30076
770-642-1000 F1\X 770-(,42-8808
as,o,
January 12, 2004 ., d''~---------<JI
" ~\_\J ? "' ~
\~ ~w.t\\'v ·,
<:,tl1t.t,,~\\
'· '.:-
,. ~ --,-~--,-l:-. ',.,
Per your request the results from the recovery and monitoring wells on your property arc provided.
The groundwater was analyzed for seven target volatile organic compounds (VOCs), one semi-volatile
organic compound (SYOC), and five metals. All field and laboratory methods utilized were approved by
the U.S. Environmental Protection Agency (EPA). The results from September 2003 for MW-64, MW-
64A, MW-66 and RWSF-l(see Figure 1) are provided in the attached laboratory reports and arc
summarized in the attached tables.
EPA requires General Electric to sample the wells quarterly as part of a long-term monitoring
plan. The groundwater will continue to be sampled for seven VOCs, and five metals. Approval by the
EPA and NCDENR has been given to reduce the quarterly sampling events to semi-annual. Measurements
will take place in the months of March and September. The one SVOC, nitrobenzene, has been removed
from the semi-annual sampling events with EPA approval. It will be sampled only during the annual
sampling events that occur in September of every year. In the event that nitrobcnzene is recovered during
the annual sampling event it will be placed back onto the list for semi-annual sampling.
We will continue to report groundwater sampling results to you as they become available. If you have any
questions, please feel free to call me at [phone] or Mr. Barry Hallock at [phone].
cc. Michael Townsend (EPA)
Barry Hallock (GELS)
David Mattison (NCDENR)
Jim Laforest (COM Federal)
Hill Resultsl2-03.doc
Sincerely,
~C{a tle11c1~
Patricia Hermann
Project Scientist
---:..---=------
P. IGE\rgvplgis-rgvp\SF s1te.wor
Expla11atio11
• Site monitor well
♦ Recovery well
.-Sampled Residential well
0 Piezometer 0
" ' RWSF-2 ♦ ..._
El
MW•62
MW'62A •
300
SCALE IN FEET
RWSF-3 .. MW.66
RWSF-4'-
TITLE:
LOCATION
~/, (:b~ 1_~ .... '-Pz.s~e
arrow~~~
habitat -·-~
BAPZ·7 0
Location of Shepherd Farm Subsite Features
600 l--------------------,;:C~HE~C~K~ED;;r;;P¼AWW--,-,~IGGIU~R~E~, 1 -G ri DRAFTED PEP
East Flat Rock, NC
.......,.._ eo rans f-FIL-E--t-c-SF-s,i,-wo-, --j 4'ffl!:t:--4. ,H,,. nc" w,.,,, • .,, , Inc. DATE 11130,01 1
• •
•
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results.
Remediation
Parameter Goal
voe, (µg/LJ
1,2-Dichlorocthane
Benzene
Chloroform
cis-1,2-Dichlurocthcne 70
Teirachloroethene
tr,ms-1.2-Dich!oroethcnc 70
Trichloroethene 2.8
Vinyl chloride
SVOCs (µg/L)
Nitrobcnzcne 10
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,NO • not detected
J • detected, estimated result
UJ • not detected, estimated result
D • dilution sample
E • exceed calibration limit
B -found in blank
NA • not analyzed
2000
4
15
50
100
MW-64
Sep-00 Dec-00 Mar-01 Jun-01 · Sep-01 Dec-01
ND(2.0) ND (2.0) ND(2.0) ND (2.0J ND(2.0) ND(2.0)
ND(\.0) ND(l.0) ND(l.O) ND(l.0) ND(l.0) ND(\.0)
1.0 J ND(2.0) ND(2.0) ND (2.0) ND(2.0J ND (2.0)
ND(2.0) ND{2.0) ND(2.0) ND(2.0) ND (2.0) ND (2.0)
3.6 2.8 0.83 J 1.9 J s.o 3.0
ND(2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0) ND(2.0)
ND (2.0) ND (2.0) ND (2.0J ND(2.0J ND(2.0) ND(2.0)
ND ( 1.0) ND(l.0) ND I 1.0) ND I I.OJ ND(l.0) ND I 1.0)
ND(5.0) ND(5.0) ND (5.5) ND (5.0) ND(5.0) ND (5.0)
37.9 B 53.0 J 20.1 J 22.0 J 37 .9 J 34.5 J
0.68 J 0.68 U 0.5( U 0.75 U 0.67 U 0.45J
1.5 J 12.7 3.4 U I.JU 1.2 u 4.7 U
8.4 J 27.7 2.7 UJ 2.7 U 3.4 UJ 7 .0 J
5.4 U 0.8 U i.2 J 0.8 U 0.8 U 0.8 U
Bolded values indicate de1ec1ed concemrations grealer than remediation goals.
Mar-02 Jun-02 Scp-02 Dcc-02
ND(2.0) ND{2.0) ND(2.0) ND(2.0)
ND(l.O) ND(l.OJ ND (1.0) ND(l.0)
ND (2.0) ND(2.0) ND (2.0) ND (2.0) • ND(2.0) ND(2.0) ND(2.0) ND (2.0)
0.54 J 1.2 J 4.0 ND(2.0)
ND (2.0) ND (2.0) ND (2.0) ND(2.0)
ND(2.0) ND (2.0) ND(2.0) ND (2.0)
ND(l.OJ ND(l.0) l\'D(l.0) ND ( 1.0)
NA NA ND (5.0) NA
36.8 J 25.6 J 55.5 J 16.8 J • 0.22 U 0.26 U 0.26 U 0.26 U
8.8 2.8 J 7.9 1.2 U
16.3 J 4.7 J 16.7 6.4 J
1.5 J I.] u I.I U 1.1 U
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results.
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroelhane
Benzene
Chlorofom1
cis-1.2-Dichloroechcnc
Tetrachlorocthene
trans-1.2-Dichloroethenc
Trichloroethene
Vinyl chloride
SVOCs (µg/L)
Nitrobcnzene
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J • detected, estimated result
UJ -not detected, estimated result
D • dilution sample
E • exceed calibration limit
B -found in blank
NA -not analyzed
70
70
2.8
10
2000
4
15
50
100
MW-64
Mar-03 Jun-03 Sep-03 Dec-03 Mar-04 Jun-04
ND (2.0) NDt2.0) ND(2.0)
ND(l.0) ND(l.0) ND(l.0)
ND (2.0) ND{2.0) ND(2.0)
ND(2.0) ND (2.0) ND(2.0)
ND (2.0) ND (2.0) ND(2.0)
ND(2.0) ND(2.0) ND(2.0)
ND (2.0) ND(2.0) ND(2.0)
ND (1.0) ND(l.0) ND I 1.0)
NA ND(50)
15.2 J 18.9 J 61.0J
1.4 J 0.26 U 0.26 U
4.7 U 1.2 u 15.7
3.4 J 1.6 J 36.8
I.I u I.I u 11.0 J
Bolded values indicate detected concentrations grea1er 1han remediation goals.
Sep-04 Dcc-04 Mar-OS Jun-OS
•
•
• • Accutest Laboratories
Report of Analysis Page I of I
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
MW-64
Fl9465-l 1
AQ -Ground Water
SW846 82608
Project: GELS, Hendersonville, NC
Run #I
Run #2
\Run #I
Run #2
File ID
G0023918.D
Purge Volume
5.0 ml
DF
I
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 1,2-Dicbloroethane
156-59-2 cis-1,2-Dichloroethylene
156-60-5 trans-1,2-Dichloroethylene
127-18-4 Tetracbloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
Analyzed By
09/17/03 JG
Result RL
ND 1.0
ND 2.0
ND 2.0
ND 2.0
ND 2.0
ND 2.0
ND 2.0
ND 1.0
Date Sampled: 09/09/03
Date Received: 09/11/03
Percent Solids: n/a
Prep Date
n/a
MDL Units
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
Prep Batch Analytical Batch
n/a VG859
Q
CAS No. Surrogate Recoveries Run# l Run#2 Limits
1868-53-7 Dibromolluoromethane 103%
17060-07-0 1,2-Dichloroethane-D4 84%
2037-26-5 Toluene-DB 98%.
460-00-4 4-Bromolluorobenzene 91 %
ND = Not detected MDL -Method Detection Limit
RL = Reponing Limit
E = Indicates value exceeds calibration range
86-115%
78-125%
87-113%
84-117%
1 = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
U ... -
..l. j
• Accutest Laboratories
Report of Analysis Page I of I
Client Sample ID: MW-64
Lab Sample ID: Fl9465-l l Date Sampled: 09/09/03
Matrix: AQ -Ground Water Date Received: 09/11/03
Method: SW846 8270C SW846 3510C Percent Solids: n/a
Project: GELS, Hendersonville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0I893I.D I 09/15/03 ME 09/ 13/03 OP8500 SLI0I6
Run#2
Initial Volume Final Volume
Run#! 1000ml 1.0 ml
Run #2
ABN TCL List
CAS No. Compound Result RL MDL Units Q
98-95-3 Nitrobenzene ND 5.0 1.0 ug/1
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 36% 19-90%
4165-62-2 Phenol-d5 24% 10-68%
118-79-6 2,4,6-Tribromophenol 78% 36-137%
4165-60-0 Nitrobenzene-d5 78% 49-119%
321-60-8 2-Fluorobiphenyl 71 % 45-118%
1718-51-0 Terphenyl-dl4 76% 46-135%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
03:
• Accutest Laboratories
Client Sample ID:
Lab Sample ID:
Matrix:
MW-64
Fl9465-II
AQ -Ground Water
•
Report of Analysis
Date Sampled: 09/09/03
Date Received: 09/ 11/03
Percent Solids: n/a
Page I of I
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units DF Prep Analyzed By Method Prep Method
Barium 61.0'Q. ~ 200 0.49 ug/1 I 09/16/03 09/18103 DM SW846 60108 SW846 3010A
Beryllium 0.26 U 5.0 0.26 ug/1 I 09/16/03 09/18103 DM SW846 60108 SW846 3010A
Lead 15,7 5.0 1.2 ug/1 I 09/16103 09/18103 DM SW846 60108 SW846 3010A Manganese 36.8 15 0.16 ug/1 I 09/16/03 09/18103 DM SW846 60108 SW846 3010A Nickel IL0"8.1' 40 I. I ug/1 I 09/16/03 09118/03 DM SW846 60108 SW846 3010A
RL = Reporting Limit
IDL = Instrument Detection Limit
U = Indicates a result < IDL
B = Indicates a result > = IDL but < RL
,...._ ') r··. •
.... , ·' .,1,1 · ..•
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1.2-Dichloroethanc
Bcnzcnc
Chlorofonn
cis-1.2-Dichlorocthcnc
Tctr.ich\oroethenc
tr.ins-1,2-Dichloroethcnc
Trichloroethcne
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND • not detected
J • detected, estimated result
UJ • not detected, estimated result
D • dilution sample
E • exceed calibration limit
B -found in blank
NA • not analyzed
70
70
2.8
10
:woo
4
15
50
100
MW-64A
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND(2.0) ND(2.0) ND(2.0) ND (2.0) ND (2.0) ND(2.U)
NO(l.0) ND(\.0) ND(l.0) ND ( 1.0) ND(l.0) ND(l.0)
ND(2.0) ND (2.0) ND(2.0) 0.68 J 0.68 J ND (2.0)
ND (2.0) ND(2.0) ND(2.0J ND (2.0) ND (2.0) ND (2.0)
S0.2 46.7 43.1 41.8 42.8 41.8
ND(2.0) ND (2.0) ND(2.0) ND(2.0) ND(2.0) ND(2.0)
ND (2.0) ND(2.0) ND (2.0) ND(2.0) ND(2.0) ND(2.0)
ND I 1.0) ND(I.0) ND I 1.0) ND(l.0) ND ( 1.0) ND I 1.0)
ND(S.0) ND(5.0) ND(5.0) ND(5.0) ND(5.0) ND(5.0)
34.0 J 33.6 J 36.0 J 32. 7 J 29.7 J 30.2 J
0.79 U 0.86 UJ 0.76 U 0.83 U 0.6 U 0.22 U
1.2 U 1.7 UJ 2.5 U 1.4 U 1.2 J 4.4 U
90.7 76.9 J 92.4J 70.8 51.4 J 50.4
1.9 U 0.8 UJ 0.97 J 0.8 U 0.8 U 0.8 U
Bolded V'Jlues indicate dctec1ed concentrations greater than remediation goals.
Mar-02 Jun-02 Scp-02 Dcc-02
ND(2.0) ND(2.0) ND(2.0) ND{2.0)
ND(\.0) ND ( I.OJ ND(\.0) Nil ( 1.0)
0.77 J 0.75 J 0.74 J 0.8 J • ND(2.0) ND(2.0) ND(2.0) ND(2.0)
43.8 37.2 36.3 29.S
ND(2.0) ND (2.0) ND(2.<J) ND(2.0)
ND (2.0) ND (2.0) ND(2.0) ND(2.0)
ND(I.0) ND(l.0) ND I 1.0) ND(\.0)
NA NA NO (5.0) NA
31.8 J 32.1 J 32.4 J 42.8 J • 0.26 U 0.26 U 0.22 U 0.26 U
2. 7 J 1.2 U 1.8 U 1.2 U
54.0J 93.-1 99.5 216
0.8 U I. I U I. I U I. I U
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation MW-64A
Parameter Goal Mar-03 Jun-03 Sep-03 Dec-03 Mar-04 Jun-04
voes (µg/L)
1,2-Dichlorocthane
Benzem:
Chlorofonn
cis-1.2-Dichloroelhene 70
Tetrachlorocthene
trans-1.2-Dichlorocthene 70
Trichlorocthcne 2.8
Vinyl chloride
SVOCs (µg/L)
Nitrobenzenc 10
METALS TOTAL (µg/L)
Barium 2000
Bcry\Jium
Lead
Manganese
Nickel
Notes:
U,NO -not detected
J -detected, estimated result
UJ -not detected, estimated result
0 • dilution sample
E -exceed calibration limit
B -found in blank
NA• not analyzed
4
15
50
100
ND(2.0) ND (2.0) ND(2.0)
ND ii.OJ ND(I.0) ND(l.01
0.65 J 0.63 J 0.51 J
ND(2.0) ND (2.0) ND{2.0)
34.9 33.7 38.0
ND(2.0) ND(2.0) ND(2.0)
ND (2.0) ND(2.0) ND(2.0)
ND(LO) Nil I 1.0) ND (1.0)
NA ND(5.0)
35.7 J 36.8 J 37.4 J
0.26 U 0.26 U 0.26 U
1.3 u 1.2 u 1.2 U
137 264 167
1.1 u I. I U I.I u
Bolded values indicate detected concentrations greater than remediation goals.
Sep-04 Dec-04 Mar-05 Jun-05
•
•
• • Accutest Laboratories
Report of Analysis Page I of I
Client Sample ID: MW-64A
Lab Sample ID: Fl9465-12 Date Sampled: 09/09/03 Matrix: AQ -Ground Water Date Received: 09/11/03
Method: SW846 8260B Percent Solids: n/a
Project: GELS, Hendersonville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #I G0023919.D 09/17/03 JG n/a n/a VG859 Run #2
IRun #I
Purge Volume
5.0 ml
Run#2
VOA TCL List
CAS No. Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 0.50 ug/1
67-66-3 Chlorofonn 0.51 2.0 0.50 ug/1 1 107-06-2 1,2-Dichloroethane ND 2.0 0.50 ug/1 156-59-2 cis-1,2-Dichloroethylene ND 2.0 0.50 ug/1
156-60-5 trans-1,2-Dichloroethylene ND 2.0 0.50 ug/1
127-18-4 Tetrachloroethylene 38.0 2.0 0.50 ug/1 79-01-6 Trichloroethylene ND 2.0 0.50 ug/1 75-01-4 Vinyl chloride ND 1.0 0.50 ug/1
CASNo. Surrogate Recoveries Run# 1 Run#2 Limits
1868-53-7 Dibromofluoromethane 101% 86-115%
17060-07-0 l ,2-Dichloroethane-D4 84% 78-125%
2037-26-5 Toluene-DB 97% 87-113%
460-00-4 4-Bromofluorobenzene 94% 84-117%
ND = Not detected MDL -Method Detection Limit 1 = Indicates an estimated value RL = Reponing Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
• Accu1es1 Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: MW-64A
Lab Sample ID: Fl9465-12 Date Sampled: 09/09/03
Matrix: AQ -Ground Water Date Received: 09/11/03
Method: SW846 8270C SW846 3510C Percent Solids: n/a
Project: GELS, Hendersonville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #l L018932.D I 09/15/03 ME 09/13/03 OP8500 SLI016
Run #2
Initial Volume Final Volume
Run #I 1000 ml 1.0 ml
Run #2
ABN TCL List
CAS No. Compound Result RL MDL Units Q
98-95-3 Nitrobenzene ND 5.0 1.0 ug/l
CAS No. Surrogate Recoveries Run# 1 Run#2 Limits
367-12-4 2-Fluorophenol 34% 19-90%
4165-62-2 Phenol-d5 23% 10-68%
118-79-6 2,4,6-Tribromophenol 71 % 36-137%
4165-60-0 Nitrobenzene-d5 72% 49-119%
321-60-8 2-Fluorobiphenyl 66% 45-118%
1718-51-0 Terphenyl-dl4 75% 46-135%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
0 0 •:: .-)
,J ,:.
• Accutest Laboratories
Client Sample ID: MW-64A
Lab Sample ID: FI 9465-12
Matrix: AQ -Ground Water
•
Report of Analysis
Date Sampled: 09/09/03
Date Received: 09/11/03
Percent Solids: n/a
Page I of I
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units DF Prep Analyzed By Method Prep Method
Barium 37_4,;i,_ ') 200 0.49 ug/1 09/16/03 09/18/03 DM SW846 6010B SW846 3010A Beryllium 0.26 U 5.0 0.26 ug/1 I 09/16/03 09/18/03 DM SW846 6010B SW846 3010A
Lead 1.2.U 5.0 1.2 ug/1 I 09/16/03 09/18/03 DM SW846 6010B SW846 3010A
Manganese 167 15 0.16 ug/1 I 09/16/03 09/18/03 DM SW846 6010B SW846 3010A Nickel I. I U 40 1.1 ug/1 I 09/16/03 09/18/03 DM SW846 6010B SW846 3010A
RL = Reporting Limit V = Indicates a result < IDL
IDL = Instrument Detection Limit B = Indicates a result > = IDL but < RL UiJ
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1.2-0ichlorocthanc
Benzene
Chlorofom1
ci~-1.2-Dichlorocthene
Tctrachloroethcnc
trnns-I ,2-Dichluroe1hcnc
T richloroethene
Vinyl chloride
SVOCs (µg/L)
Niirobcnzcnc
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND • not detected
J -detected, estimated result
UJ -not detected, estimated result
D • dilution sample
E -exceed calibration limit
B -found in blank
NA -not analyzed
70
70
2.8
10
2000
4
15
50
100
MW-66
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND(2.0) ND(2.0) ND (2.0) ND (2.0) ND(2.0) ND (2.0)
ND(l.0) ND(l.0) ND(l.0) ND(l.0) ND ( 1.0) ND(l.0)
ND(2.0) ND (2.0) 0.81 J ND(2.0) 0.77 J ND(2.0J
1.6 J ND (2.0) ND(2.01 ND (2.0) ND(2.0) ND(2.0)
23.2 J 45.8 53.4 54.5 65.7 58.5
ND (2.0) ND(2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0)
0.94 J ND(2.0) ND (2.0) ND{2.0) ND (2.0) ND (2.0J
ND(I.OJ ,<DI I.OJ ND ( 1.0) ND ii.OJ ND(I.OJ ND(I.OJ
ND(5.0J ND (5.0J ND (5.SJ ND (5.0J ND (5.0J ND (5.0)
52.J J 36.1 J 39.6 J 26.0 J 40.0 J 39.2 J
1.5 u 0.87 UJ 0.8 U 0.94 U 0.81 U 0.22 U
4.2 J 1.6 UJ 3.8 U 1.6 U 1.9 J 6.3 U
223 57.3 J 81.2 20.4 119.0J 98.9
5.3 U 1.8 J 1.8 U 0.8 U 1.2 J 1.9 J
Bolded values indicate detected concentralions greater than rcmedia1ion goals.
Mar-02 Jun-02 Sep-02 Dcc-02
ND (2.0) ND(2.0) ND(2.0) ND(2.0)
ND(l.0) ND(l.0) ND(\.0) ND(l.0)
0.85 J 0.65 J 0.69 J 0.7 J • ND(2.0) 0.52 J 0.55 J ND(2.0)
61.1 64.8 71.J 76.6
ND(2.0) ND(2.0) ND(2.0) ND 12.0)
ND (2.0) ND(2.0) ND (2.0) ND(2.0)
ND ( 1.0) ND(I.OJ ND(l.OJ ND(LO)
NA NA ND (5.0) NA
28.0 J 26.5 J 30.8 J 28.9 J • 0.22 U 0.26 U 0.26 U 0.26 U
2.5 J 1.2 u 2.5 U 1.2 U
16.4 J 25.9 45.0 38.8
0.8 U I.! u I.I U 1.1 U
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation MW-66
Parameter Goal Mar-03 Jun-03 Sep-03 Dec-03 Mar-04 Jun-04
voes (µg/L)
1,2-Dichlorocthane
Benzene
Chlorofonn
ci;.-l ,2-Dichlorocthene 70
Tetrnchlorocthene
trnns-1,2-Dichloroethcne 70
Trichlorocthcne 2.8
Vinyl chloride
SVOCs (µg/L)
Nitrobenzcne 10
METALS TOT AL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J • detected, estimated result
UJ • not detected, estimated result
D -dilution sample
E -exceed calibration limit
B -found in blank
NA• not analyzed
2000
4
15
50
100
ND(2.0) ND(2.Q) ND (2.0)
ND ( 1.0) ND(l.01 ND(L0)
0.661 0.59 J 0.69 J
0.89 J 0.79 J 0.97 J
80.2 83.0 76.6
ND(2.0) ND(2.0) ND(2.0)
ND(2.0) ND(2.0) ND (2.0)
ND(l.0) ND(I.0) ND(l.0)
NA ND(5.0)
22.5 J 22.8 J 22.7 J
0.26 U 0.26 U 0.26 U
1.4 U 1.2 u 1.2 u
6.6 J 14.1 J 5.9 J
I.I U I.I u (.] u
Boldcd values indicate detected concentrations greater than remediation goals.
Sep-04 Dec-04 Mar-05 Jun-05
•
•
• • Accu,est LaboralOries
Report of Analysis Page I of I
Client Sample ID: MW-66
Lab Sample ID: Fl9465-13 Date Sampled: 09/09103 Matrix: AQ -Ground Water Date Received: 09/11/03 Method: SW846 8260B Percent Solids: n/a Project: GELS, Hendersonville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #I G0023920.D I 09117103 JG n/a n/a VG859 Run #2
IRun #I
Purge Volume
5.0 ml
Run #2
VOA TCL List
CAS No. Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 0.50 ug/1 67-66-3 Chlorofonn 0.69 2.0 0.50 ug/1 ] l07-06-2 1,2-Dichloroethane ND 2.0 0.50 ug/1 156-59-2 cis-1,2-Dichloroethylene 0.97 2.0 0.50 ug/1 ] 156-60-5 trans-1,2-Dichloroethylene ND 2.0 0.50 ug/1 127-18-4 Tetrachloroethylene 76.6 2.0 0.50 ug/1 79-01-6 Trichloroethylene ND 2.0 0.50 ug/1 75-01-4 Vinyl chloride ND 1.0 0.50 ug/1
CAS 1-io. Surrogate Recoveries Run# 1 Run#2 Limits
1868-53-7 Dibromofluoromethane 100% 86-115% 17060-07-0 1,2-Dichloroelhane-D4 86% 78-125% 2037-26-5 Toluene-DB 100% 87-113% 460-00-4 4-Bromofluorobenzene 94% 84-117%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound
0 ·~ .. ·, '-,:.,,
•
Accutest Laboratories
Report of Analysis Page I of I
Client Sample ID: MW-66
Lab Sample ID: F!9465-13 Date Sampled: 09109103
Matrix: AQ -Ground Water Date Received: 09/11/03
Method: SW846 8270C SW846 3510C Percent Solids: n/a
Project: GELS, Hendersonville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0!8933.D I 09/15/03 ME 09/13/03 OP8500 SL10!6
Run #2
Initial Volume Final Volume
Run #I 1000ml 1.0ml
Run#2
ABN TCL List
CAS No. Compound Result RL MDL Units Q
98-95-3 Nitro benzene ND 5.0 1.0 ug/1
CASNo. Surrogate Recoveries Run# I Run#2 Limits
367-12-4 2-Fluorophenol 39% 19-90%
4165-62-2 Phenol-d5 26% 10-68%
118-79-6 2,4,6-Tribromophenol 77% 36-137%
4165-60-0 Nitrobenzene-<15 79% 49-119%
321-60-8 2-Fluorobiphenyl 71 % 45-118%
1718-51-0 Terphenyl-dl4 79% 46-135%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reponing Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
•
Accutest Laboratories
Client Sample ID: MW-66
Lab Sample ID: f 19465-13
Matrix: AQ -Ground Water
Report of Analysis
Date Sampled: 09/09/03
Date Received: 09/11/03
Percent Solids: n/a
Page I of I
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units DF Prep Analyzed By Method Prep Method
Barium 22.7'B,, > 200 0.49 ug/1 I 09/16/03 09/18/03 DM SW846 60l0B SW846 3010A
Beryllium 0.26 U 5.0 0.26 ug/1 1 09/16/03 09/18/03 DM SW846 6010B SW846 3010A
Lead 1.2.U 5.0 1.2 ug/1 I 09/16/03 09/18/03 DM SW846 60l0B SW846 3010A
Manganese 5,9'§;..,'. 15 0.16 ug/1 I 09/16/03 09/18/03 DM SW846 60l0B SW846 3010A
Nickel LIU 40 I. 1 ug/1 I 09/16/03 09/18/03 DM SW846 60l0B SW846 3010A
RL = Reporting Limit U = Indicates a result < IDL
ID L = Instrument Detection Limit B = Indicates a result > = IDL bu! < RL
0
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voe, (µg/LJ
l ,2-Dichloroethanc
Benzene
Chlorofonn
cis-1.2-Dichloroethcne
Tetrnchlorocthcne
mms-1,2-Dichloroethcnc
Trichloroethcnc
Vinyl chloride
SVOCs (µg/L)
Nitrobcn;,enc
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Mangane~c
Nickel
Notes:
U,ND • not detected
J • detected, estimated result
UJ • not detected, estimated result
0 -dilution sample
E -exceed calibration limit
B -found in blank
NA -not analyzed
70
70
2.8
10
2000
4
15
50
100
RWSF-1
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND(2.0) ND(2.0) NU (2.0) ND(2.0) ND(2.0) ND(2.0)
ND(l.0) ND(l.0) ND(l.0) ND(l.0) ND(!.0) ND ( 1.0)
ND(2.0) ND(2.0) ND(2.0) ND (2.0) ND(2.0) ND(2.0)
ND (2.0) ND(2.Q) ND(2.0) ND(2.0) ND(2.0) ND (2.0)
34.0 51.4 43.2 0 40.4 46.3 52.6
ND(2.0) ND(2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0)
ND(2.0) ND (2.0) ND(2.0) ND(2.0) ND(2.0) ND (2.0)
ND ( 1.0) ND(\.0) ND(I.O) ND(I.0) ND ( 1.0) ND I I.OJ
ND (5.0) ND(5.0) ND (5.5) ND (5.5) ND(5.0) ND(5.0)
161.0J 193.0 J 290 242.0 254.0 J 153.0 J
0.3 U 2.6 UJ 2.2 U 2.3 U I.I J 1.2 J
1.5 J 50.6 J 49.5 21.4 24.3 10.4 U
65.6 42.6 J 109.0J 100.0 90.1 J 71.SJ
I 3. 7 J 1.4 J 6.5 J 0.8 U 3.5 J 1.8 j
Bolded values indicate de1ected concentrations greater than remediacion goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND(2.0) ND (2.0) ND (2.0)
ND (1.0) ND(l.01 ND f 1.0) ND f 1.0)
0.52 J ND (2.0) 0.52 J ND (2.0) • ND (2.0) ND(2.0) ND(2.Q) ND(2.0)
56.3 56.-1 43.2 63.6
ND (2.0) ND{2.0) ND(2.0) ND{2.0J
ND (2.0) ND tz.0) ND(2.0) ND{2.0)
ND(l.0) ND(l.0) ND ( 1.0) ND(l.0)
NA NA ND(5Jl) NA
156.0 J 142.0 J 134.0 J 61.3 J • Q.22 U 0.26 U 0.26 U 0.26 U
26.1 22.7 18.4 1.2 U
98.1 J l05 77.6 0.16 U
4.2 J I. I U I.I u I.I u
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1.2-Dichloroethane
Benzene
Ch\orofonn
cis-l ,2-Dichloroe1hcnc 70
Tetrachloroelhene
tmns-1,2-0ichlorocthene 70
Trichloroclhcne 2.8
Vinyl chloride
SVOCs (µg/L)
Nitrobcnzene 10
METALS TOT AL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,NO -not detected
J • detected, estimated result
UJ • not detected, estimated result
D • dilution sample
E -exceed calibration limit
B -found in blank
NA -not analyzed
2000
4
15
50
100
RWSF-1
Mar-03 Jun-03 Sep-03 Dec-03 Mar-04 Jun-04
ND(2.0) ND(2.0) ND (2.0)
ND (\.0) ND(l.0) ND (I.OJ
ND (2.0) ND(2.0) ND (2.0)
ND(2.0) ND(2.0) 3.5
32.2 38.1 37.7
ND(2.0) ND(2.0) ND(2.0)
NO (2.0) ND(2.0) 0.91 J
ND(l.0) ND(l.0) ND ( 1.0)
NA ND(5.0)
28.3 J 47.6 J 152.0 J
0.26 U 0.26 U 0.26 U
30.5 106 7.9
12.8 J 126 64.5
311 100.0 1.8 J
Boldcd values indicate detected concentrations greater than remediation goals.
Sep-04 Dec-04 Mar-05 Jun-05
•
•
• Accutest Laboratories
Report of Analysis Page I of I
Client Sample ID: RWSF-1
Lab Sample ID: F19472-6 Date Sampled: 09/10/03
Matrix: AQ -Ground Water Date Received: 09/12/03
Method: SW846 8260B Percent Solids: n/a
Project: GELS, Hendersonville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 G0023950.D I 09/18/03 JG n/a n/a VG860
Run #2
IRun #I
Purge Volume
5.0 ml
Run #2
VOA TCL List
CAS No. Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 0.50 ug/1
67-66-3 Chloroform ND 2.0 0.50 ug/1
107-06-2 1,2-Dichloroethane ND 2.0 0.50 ug/1
156-59-2 cis-1,2-Dichloroethylene 3.5 2.0 0.50 ug/l
156-60-5 trans-l ,2-Dichloroethylene ND 2.0 0.50 ug/l
127-18-4 Tetrachloroethylene 37.7 2.0 0.50 ug/l
79-01-6 Trichloroethylene 0.91 2.0 0.50 ug/1 J
75-01-4 Vinyl chloride ND 1.0 0.50 ug/l
CASNo. Surrogate Recoveries Run# 1 Run#2 Limits
1868-53-7 Dibromofluoromethane 101 % 86-115%
17060-07-0 1,2-Dichloroethane-D4 82% 78-125%
2037-26-5 Toluene-D8 99% 87-l [3%
460-00-4 4-Bromofluorobenzene 92% 84-117%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
0 C.,0 . o·, , . ., ~----..L'
• Accutest Laboratories
Report of Analysis Page I of I
Client Sample ID: RWSF-1
Lab Sample ID: Fl9482-8 Date Sampled: 09/10/03
Matrix: AQ -Ground Water Date Received: 09/12/03
Method: SW846 8270C SW846 35IOC Percent Solids: n/a
Project: GELS, Hendersonville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #I LOI8987.D I 09/19/03 ME 09/17/03 OP8521 SL1020
Run#2
Initial Volwne Final Vol wne
Run #I 1000ml 1.0 ml
Run #2
ABNTCL List
CAS No, Compound Result RL '.\<IDL Units Q
98-95-3 Nitrobenzene ND 5.0 1.0 ug/1
CAS No. Surrogate Recoveries Run# I Run# 2 Limits
367-12-4 2-Fluorophenol 51 % 19-90%
4165-62-2 Phenol-d5 34% 10-68%
118-79-6 2,4,6-Tribromophenol 84% 36-137%
4165-60-0 Nitrobenzene-d5 84% 49-119%
321-60-8 2-Fluorobiphenyl 74% 45-118%
1718-51-0 Terphenyl-dl4 81 % 46-135%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value
RL = Reponing Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
01
• Accutest Laboratories
Client Sample ID: RWSF-1
Lab Sample ID: Fl9482-8
Matrix: AQ -Ground Water
Report of Analysis
Date Sampled: 09/10/03
Date Received: 09/ 12/03
Percent Solids: n/a ·
Page l of l
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units DF Prep Analyzed By Method Prep Method
Barium 152 a_} 200 0.49 ug/1 09/16/03 09/18/03 DM SW846 60l0B SW846 3010A
Beryllium 0.26 U 5.0 0.26 ug/1 09/16/03 09/18/03 DM SW846 60l0B SW846 3010A
Lead 7.9 5.0 1.2 ug/1 09/16/03 09/18/03 DM SW846 60l0B SW846 3010A
Manganese 64.5 15 0.16 ug/1 09/16/03 09/18/03 DM SW846 60l0B SW846 3010A
Nickel l.8'B;."j" 40 I.I ug/1 09/16/03 09/18/03 DM SW846 60l0B SW846 3010A
RL = Reporting Limit U = Indicates a result < IDL
IDL = Instrument Detection Limit B = Indicates a result > = IDL but < RL
Geo• . ATETRATECHCOMPAH~lrans, Inc.
' • www.geotransinc.com
Dr. Gary Hi II
250 Old TyTy Road
Tifton, GA 31794-6607
Reference:
Dear Dr. Hill:
Groundwater Sampling Results
March 2003
GeoTrans Project No. 2204.028.41
• C,/E'
1 080 Holcomb Bridge Road
Building 100, Suite 190
Roswell, GA 30076
770-642-1000 F1\X 770-642-BS0B
2 ·2 2003
May 19, 2003 '
Per your request the results from the recovery and monitoring wells on your property are
provided. The groundwater was analyzed for seven target volatile organic compounds (VOCs),
and five metals. All field and laboratory methods utilized were approved by the U.S.
Environmental Protection Agency (EPA). The results from March 2003 for MW-64, MW-64A,
MW-66 and RWSF-l(see Figure I) are provided in the attached laboratory reports and are
summarized in the attached tables.
EPA requires General Electric to sample the wells quarterly as part of a long-term
monitoring plan. The groundwater will continue to be sampled for seven VOCs, and five metals.
The one SVOC, nitrobenzene, has been removed from the quarterly sampling events with EPA
approval. It will be sampled only during the annual sampling events that occur in September of
every year. In the event that nitrobenzene is recovered during the annual sampling event it will be
placed back onto the list for quarterly sampling. We will report groundwater sampling results to
you as they become available. If you have any questions, please feel free to call me at (770) 642-
1000 or Mr. Lee Humphrey at [phone].
cc. Michael Townsend (EPA)
Lee Humphrey (GELS)
David Mattison (NCDENR)
P:\GE\DOCS\RESIDEN1\HILL RF..SUL TS\Hill Rc~ults03-03,wpd
May 19, 2003
Sincerely,
~Cid-lk/µ.-(CU,Ut__
Patricia Hermann
Project Scientist
P :\GE\rgvp\gis-rgvp\SF site. wo,:
! r--------1--
--__ , __
Expla11atio11
• Site monitor well
♦ Recovery well
-+-Sampled Residential well
0 Piezometer
n
0
RWSF-2 ♦ _.._
300
SCALE IN FEET
RWSF-3 .. MW-66
RWSF-4'°
TlnE:
LOCATION:
~.~ ~
""''·'iun~~ arrowhe Q
habitat
BAPZ-7 0
Location of Shepherd Farm Subsite Features
East Flat Rock, NC
600 .----------------,-,--~---~------I ~GeoT ~:;:~::; FIGURE:
a ◄ A rE1HA rfCH COMPAi/~ Ir ans, Inc. >,-IL-.--<-S-F-sit-,-w-~--
OATE 11/30/01
1
Shepherd Farm Subsite -Performance Well Analytical Results.
Remediation
Parameter Goal
voes (µg/LJ
1,2-Dichloroethane
Benzene
Chloroform
cis-1,2-Dichloroethene 10
Tetrachloroethene
trans-1,2-Dichloroethene 10
Trichloroethene 2.8
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene 10
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,NO -not detected
J -detected, estimated result
UJ -not detected, estimated result
D -dilution sample
E -exceed calibration limit
B -found In blank
NA -not analyzed
2000
4
15
50
100
MW-64
Sep-00 Dcc-00 Mar-01 Jun-01 Scp-01 Dec-01
ND (2.0) ND (2.0J ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0)
1.0 J ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0) ND(2.0)
3.6 2.8 0.83 J 1.9 J 5.0 3.0
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0J ND (2.0)
ND (2.0) . ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0)
ND (5.0) ND(5.0) ND (5.5) ND (5.0) ND (5.0) ND (5.0)
37.9 8 53.0 J 20.1 J 22.0 J 37.9 J 34.5 J
0.68 J 0.68 U 0.51 U 0.75 U 0.67 U 0.45 J
1.5 J 12.7 3.4U 1.3 u 1.2 u 4.7 U
8.4 J 27.7 2.7 UJ 2.7 U 3.4 UJ 7.0 J
5.4U 0.8 U 1.2 J 0.8 U 0.8 U 0.8 U
Balded values indicate detected concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dcc-02
ND (2.0) ND(2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) • ND (2.0) ND (2.0) ND (2.0) ND (2.0)
0.54 J 1.2 J 4.0 ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND(2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND(l.0) ND (1.0)
NA NA ND (5.0) NA
36.8 J 25.6 J 55.5 J 16.8 J • 0.22 U 0.26 U 0.26 U 0.26 U
8.8 2.8 J 7.9 1.2 U
16.3 J 4.7 J 16.7 6.4 J
1.5 J I. I U I. I U I.I u
Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation MW-64
Parameter Goal Mar-03 Jun-03 Sep-03 Dec-03 Mar-04 Jun-04
voes (µg/L)
1,2-Dichloroethane ND (2.0)
Benzene ND (1.0)
Chlorofonn ND (2.0)
cis• l ,2-Dichloroethene 70 ND (2.0)
Tetrachloroethene ND (2.0)
trans-1,2-Dichloroethene 70 ND (2.0)
Trichloroethene 2.8 ND (2.0)
Vinyl chloride ND (1.0)
SVOCs (µg/L)
Nitrobenzene NA
METALS TOTAL (µg/L)
Barium 2000 15.2 J
Beryllium 4 1.4 J
Lead 15 4.7 U
Manganese 50 3.4 J
Nickel 100 I.JU
Notes: Balded values indicate detected concentrations greater than remediation goals.
U,ND • not detected
J -detected, estimated result
UJ -not detected, estimated result
D -dilution sample
E -exceed callbration limit
B -found In blank
NA• not analyzed
Sep-04 Dec-04 Mar-OS Jun-OS
•
•
Accutest Laboratories • • Report of Analysis Page 1 of I
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
MW-64
F\6984-2
AQ -Ground Water
SW846 8260B
Project: GELS, Hendersonville, NC
Run#!
Run#2
!Run #I
Run #2
File ID
C00l5111.D
Purge Volume
5.0 ml
DF
1
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chlorofonn
107-06-2 1.2-Dichloroethane
156-59-2 cis-1,2-Dichloroethylene
156-60-5 trans-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
Analyzed By
03/25/03 KW
Result RL
ND . 1.0
ND 2.0
ND 2.0
ND 2.0
ND 2.0
ND 2.0
.ND . 2.0 ND. . 1.0
Date Sampled:
Date Received:
Percent Solids:
03/15/03
03/18/03
n/a
Prep Date
n/a
Prep Batch
n/a
MDL Units Q
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
Analytical Batch
VC665
CAS No. Surrogate Recoveries Run# 1 Run#2 Limits
1868-53-7 Dibromotluoromethane 99%
17060-07-0 l ,2-Dichloroethane-D4 106%
2037-26-5 Toluene-D8 103%
460-00-4 4-Bromotluorobenzene 105%
ND = Not detected MDL· Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range
86-115%
78-125%
87-113%
84-117%
J = Indicates an estimated value
B = Indicates analyte found in associOO,Q~
N = Indicates presumptive evidence of a compound
010
Accutest Laboratories •
Client Sample ID:
Lab Sample ID:
Matrix:
MW-64
Fl6984-2
AQ -Ground Water
Report of Analysis
Date Sampled: 03/15/03
Date Received: 03/ 18/03
Percent Solids: n/a
Page 1 of 1
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units DF Prep Analyzed By Method Prep Method
Barium 15.2-B..,_ j 200 0.49 ug/l 03/19/03 03/20/03 DM SW846 6010B SW846 3010A
Beryllium l.4'!3---j 5.0 0.26 ug/1 03/19/03 03/20/03 DM SW846 6010B SW846 3010A
Lead 4.7 B----..,. \)5.0 1.2 ug/1 03/19/03 03/20/03 DM SW846 6010B SW846 3010A
Manganese 3 .4 B---...,... 15 0.16 ug/1 03/19/03 03/20/03 DM SW846 6010B SW846 J0I0A
Nickel I. I U ,
40 I. I ug/1 03/19/03 03/20/03 DM SW846 6010B SW846 3010A
RL = Reponing Limit
IDL = Instrument Detection Limit
U = Indicates a result < IDL I\OOI\
B = Indicates a result > = IDL bf,f"~.15
013
Shepherd Farm Subsite • Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Benzene
Chloroform
cis-1,2-Dichloroethene 70
Tetrachloroethene
trans-1,2-Dichloroethene 70
Trichloroethene 2.8
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene 10
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J • detected, estimated result
UJ -not detected, estimated result
D -dllution sample
E • exceed callbratlon llmlt
B -found In blank
NA -not analyzed
2000
4
15
50
100
MW-64A
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0)
ND(2.0) ND (2.0) ND (2.0) 0.68 J 0.68 J ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
50.2 46.7 43.1 41.8 42.8 41.8
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND(2.0)
ND(2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND(l.0) ND (1.0) ND ( 1.0) ND (1.0)
ND(5.0) ND (5.0) ND (5.0) ND (5.0) ND (5.0) ND (5.0)
34.0 J 33.6 J 36.0 J 32.7 J 29.7 J 30.2 J
0.79 U 0.86 UJ 0.76 U 0.83 U 0.6 U 0.22 U
1.2U 1.7 UJ 2.5 U 1.4U 1.2 J 4.4 U
90.7 76.9 J 92.4 J 70.8 51.4 J 50.4
1.9 U 0.8 UJ 0.97 J 0.8 U 0.8 U 0.8 U
Balded values indicate detected concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND(l.0) ND(l.0) ND (1.0) ND(I.0)
0.77 J 0.75 J 0.74 J 0.8 J • ND (2.0) ND(2.0) ND (2.0) ND (2.0)
43.8 37.2 36.3 29.5
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND(l.0) ND (1.0) ND (1.0) ND (1.0)
NA NA ND (5.0) NA
J 1.8 J 32.1 J 32.4 J 42.8 J • 0.22 U 0.26 U 0.26 U 0.26 U
2.7 J 1.2 u 1.8 U 1.2 u
54.0 J 93.4 99.5 216
0.8 U I. I U I.I u I.I U
Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation MW-64A
Parameter Goal Mar-03 Jun-03 Sep-03 Dec-03 Mar-04 Jun-04
voe, (µg/L)
1,2-Dichlorocthane ND (2.0)
Benzene ND (1.0)
Chlorofonn 0.65 J
cis-I ,2-Dichloroethene 70 ND (2.0)
Tetrachloroethene 34.9
trans-1,2-Dichlorocthene 70 ND (2.0)
Trichloroethene 2.8 ND (2.0)
Vinyl chloride ND (1.0)
SVOCs (µg/L)
Nitrobenzene JO NA
METALS TOTAL (µg/L)
Barium 2000 35.7 J
Beryllium 4 0.26 U
Lead 15 l.JU
Manganese 50 137
Nickel JOO I.I u
Notes: Bolded values indicate detected concentrations greater than remediation goals.
U,NO -not detected
J -detected, estimated result
UJ -not detected, estimated result
D -dilution sample
E -exceed calibration llmlt
B -found In blank
NA -not analyzed
Sep-04 Dcc-04 Mar-OS Jun-OS
•
Accatest Laboratories •
Report of Analysis Page I of 1
Client Sample ID: MW-64A
Lab Sample ID: F16984-3
Matrix: AQ -Ground Water
Method: SW846 8260B
Project: GELS. Hendersonville, NC
Run#!
Run#2
\Run #1
Run #2
File ID
COOl5112.D
Purge Volume
5.0 ml
DF
I
VOA TCL List
C.!-..~ !'Jc. Ca::1.po:.mC
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 1,2-Dichloroethane
156-59-2 cis-1,2-Dichloroethylene
156-60-5 trans-1,2-Dichlornethylene
127-18-4 Tetrachloroeth y lene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
17060-07-0 1,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromot1uorobenzene
Analyzed
03/25/03
Res:..:.!t
NI):, .. ·•
0.65
ND
ND.'
ND
34,9 ..
ND
ND
Run# 1
98%
105%
103%
106%
Date Sampled: 03/15/03
Date Received: 03/18/03
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
KW n/a n/a VC665
!'~ '"'' YT-: .. ~ " •• "-4..1 .... ......... ~.:. ',l
·.•.··•. 1.0 0.50 ug/1
2.0 0.50 ug/1 J
2.0 0.50 ug/1
2.0 0.50 ug/1
: 2.0 0.50 ug/1
2.0 0.50 ug/1
.. 2.0 0.50 ug/1
. 1.0 0.50 ug/1
Run#2 Limits
86-115%
78-125%
87-113%
84-117%
ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associ~rn•!i~
N = Indicates presumptive evidence ~~ 11
Accutest Laboratories •
Client Sample ID:
Lab Sample ID:
Matrix:
MW-64A
FI6984-3
AQ -Ground Water
Report of Analysis
Date Sampled: 03/15/03
Date Received: 03/18/03
Percent Solids: n/a
Page I of I
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units DF Prep Analyzed By Method Prep Method
Barium 35.711-._;j 200 0.49 ug/1 I 03/19/03 03/20/03 DM SW846 6010B SW846 3010A
Beryllium 0.26.U.~ 5.0 0.26 ug/1 I 03/19/03 03/20/03 DM SW846 6010B SW846 3010A
Lead .. ·. V
1.2 ug/1 I 03/19/03 03/20/03 l.31l--.. 5.0 DM SW846 6010B SW846 3010A
Manganese 137 15 0.16 ug/1 03/19/03 03/20/03 DM SW846 6010B SW846 3010A
Nickel I.I u 40 I. I ug/1 03/ 19/03 03/20/03 DM SW846 6010B SW846 3010A
RL = Reporting Limit U = Indicates a result < IDL
IDL = Instrument Detection Limit B = Indicates a result>= IDL b'Otft)o~f
4
Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voe, (µg/LJ
1.2-Dichloroethane
Ben7..ene
Chloroform
cis-1,2-Dichloroethene 70
Tetrachloroethene
trans-1,2-Dichloroethene 70
Trichloroethene 2.8
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene 10
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J -detected, estimated result
UJ -not detected, estimated result
D -dilution sample
E • exceed callbraUon llmlt
B .found In blank
NA -not anatyzed
2000
4
15
50
100
MW-66
Sep-00 Dcc;00 l\lar-01 Jun-01 Sep-01 Dcc-01
ND (2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND(l.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0)
ND (2.0) ND(2.0) 0.81 J ND (2.0) 0.77 J ND (2.0)
1.6 J ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
23.2 J 45.8 53.4 54.5 65.7 58.5
ND(2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
0.94 J ND (2.0) ND (2.0) ND (2.0) ND(2.0) ND (2.0)
ND(l.O) ND (1.0) ND (I.OJ ND(l.0) ND (1.0) ND (1.0)
ND (5.0) ND (5.0) ND (5.5) ND (5.0) ND(5.0) ND (5.0)
52.3 J 36.1 J 39.6 J 26.0 J 40.0 J 39.2 j
1.5 u 0.87 UJ 0.8 U 0.94 U 0.81 U 0.22 U
4.2 J 1.6 UJ 3.8 U 1.6 U 1.9 J 6.3 U
223 57.3 J 81.2 20.4 119.0 J 98.9
5.3 U 1.8 J 1.8 U 0.8 U 1.2 J 1.9 J
Balded values indicate detected concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND(I.O) ND (1.0) ND (1.0)
0.85 J 0.65 J 0.69 J 0.7 J • ND (2.0) 0.52 J 0.55 J ND (2.0)
61.1 64.8 71.3 76.6
ND(2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND(2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0)
NA NA ND (5.0) NA
28.0 J 26.5 J 30.8 J 28.9 J • 0.22 U 0.26 U 0.26 U 0.26 U
2.5 J 1.2U 2.5 U 1.2 U
16.4 J 25.9 45.0 38.8
0.8 U LIU I.I u 1.IU
Shepherd Farm Subsite • Performance Well Analytical Results. (continued)
Remediation MW-66
Parameter Goal Mar-03 Jun-03 Sep-03 Dec-03 Mar-04 Jun-04
voe, (µg/LJ
1,2-Dichloroethane ND (2.0)
Benzene ND (LO)
Chlorofonn 0.66 1
cis-1,2-Dichloroethene 70 0.89 J
Tetrachloroethene 80.2
trans-1,2-Dichlorocthene 70 ND (2.0)
Trichloroethene 2.8 ND (2.0)
Vinyl chloride ND (LO)
SVOCs (µg/L)
Nitrobenzene 10 NA
METALS TOTAL (µg/L)
Barium 2000 22.5 J
Beryllium 4 0.26 U
Lead 15 1.4 U
Manganese 50 6.6 J
Nickel 100 I. I U
Notes:
U,ND -not detected
Balded values indicate detected concentrations greater than remediation goals.
J • detected, estimated result
UJ • not detected, estimated result
D • dilution sample
E -exceed calibration limlt
B -found In blank
NA -not analyzed
Sep-04 Dec-04 Mar-OS Jun-OS
•
•
Accutest Laboratories • Report of Analysis Page l of l
Client Sample ID: MW-66
Lab Sample ID: Fl6984-I
Matrix: AQ -Ground Water
Metbod: SW846 8260B
Project: GELS, Hendersonville, NC
Run #1
Run#2
File ID
C00l51 I0.D
Purge Volume
5.0 ml
DF
I
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 l ,2-Dichloroethane
156-59-2 cis-l ,2-Dichloroethylene
156-60-5 trans-l ,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Dibromotluoromethane
l 7060-07-0 l ,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromot1uorobenzene
Analyzed
03/25/03
Result
ND
0.66
ND
0.89
ND
80,2'
ND
ND
Run# 1
99%
104% ·
103% ·
l06%
Date Sampled: 03/14/03
Date Received: 03/18/03
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
KW n/a n/a VC665
RL MDL Uni!s Q
1.0 0.50 ug/l
•·. 2.0 0.50 ug/l J
\ 2.0 0.50 ug/1
.·, 2.0 0.50 ug/l J
i 1.0 0.50 ug/1
\2.0 0.50 ug/l
:, , 2.0 0.50 ug/l
1.0_ 0.50 ug/l
Run# 2 Limits
86-115%
78-125%
87-113%
84-117%
ND = Not detected MDL -Method Detection Limit J = lndicl!es an estimated value
RL = Reponing Limit
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidenQi)~d
009
Accutest Laboratories •
Client Sample ID:
Lab Sample ID:
Matrix:
MW-66
Fl6984-1
AQ -Ground Water
Report of Analysis
Date Sampled:
· Date Received:
Percent Solids:
03/14/03
03/18/03
n/a
Page l of l
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units OF Prep Analyzed By Method Prep Method __..
Barium 22.sa... > 200 0.49 ug/1 1 03/19/03 03/20/03 DM SW846 6010B SW846 3010A Beryllium 0.26 U 5.0 0.26 ug/1 I 03/19/03 03/20/03 DM SW846 60!0B SW846 3010A Lead 1,<i ~ "5.vs.o 1.2 ug/1 I 03/19/03 03/20/03 DM SW846 6010B SW846 3010A Manganese 1:{~Jn!~ 0.16 ug/1 1 03/ 19/03 03/20/03 DM SW846 60108 SW846 3010A Nickel I. I ug/1 03/19/03 03/20/03 DM SW846 60!08 SW846 3010A
RL = Reporting Limit
ID L = Instrument Detection Limit
U = lndicates a result < ID L
B = Indicates a result > = mOQQ(i}d,3
012
Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Benzene
Chloroform
cis-1,2-Dichloroethene 70
Tetrachloroethene
trans-1,2-Dichloroethene 70
Trichlomethene 2.8
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene 10
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND • not detected
J -detected, estimated result
UJ -not detected, estimated result
0 -dllutlon sample
E • exceed calibration llmlt
B -found In blank
NA -not anafyzed
2000
4
15
50
100
RWSF-1
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND(2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (I.OJ ND (I.OJ
ND (2.0) ND (2.0J ND (2.0) ND (2.0) ND(2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0J
34.0 51.4 43.2 0 40.4 46.3 52.6
ND (2.0) ND(2.0) NIJ (2.0) ND(2.0) NIJ (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND(l.O) ND (1.0) ND(l.O)
ND (5.0) ND (5.0) ND (5.5) ND (5.5) ND (5.0) ND(5.0)
161.0 J 193.0 J 290 242.0 254.0 1 153.0 J
0.3 U 2.6 UJ 2.2 U 2.3 U I.I J 1.2 J
1.5 } 50.6 J 49.S 21.4 24.3 10.4 U
65.6 42.6 J 109.0 J 100.0 90.1 J 71.8 J
13.7 J 1.4 J 6.5 J 0.8 U 3.5 J 1.8 J
Balded values indicate detected concentrations greater than remediation ~oals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND(2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0)
0.52 J ND(2.0) 0.52 J ND (2.0) • ND (2.0) ND (2.0) ND (2.0) ND (2.0)
56.3 56.4 43.2 63.6
ND (2.0) NIJ (2.0) ND (2.0) NIJ (2.0)
ND (2.0) ND(2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0)
NA NA ND (5.0) NA
156.0 J 142,0 J 134.0 J 61.3 J • 0.22 U 0.26 U 0.26 U 0.26 U
26.1 22.7 18.4 1.2 U
98.1 J 105 77.6 0.16 U
4.2 J I. I U I.I u I.JU
Shepherd Farm Subsite -Performance Well Analytical Results.
Remediation RWSF-1
Parameter Goal Mar-O3 Jun-O3 Sep-OJ Dec-O3 Mar-O4 Jun-O4
voes (µg/L)
1,2-Dichloroethane ND (2.0)
Benzene ND(I.0)
Chloroform ND (2.0)
cis-1,2-Dichloroethene 70 ND (2.0)
Tetrachloroethene 32.2
trans-1,2-Dichloroethene 70 ND (2.0)
Trichloroethene 2.8 ND (2.0)
Vinyl chloride ND (1.0)
SVOCs (µg/L)
Nitrobenzene NA
METALS TOTAL (µg/L)
Barium 2000 28.3 J
Beryllium 4 0.26 U
Lead 15 30.5
Manganese 50 12.8 J
Nickel 100 311
Notes: Balded values indicate detected concentrations greater than remediation goals.
U,ND -not detected
J -detected, estimated result
UJ • not detected, estimated result
0 -dilution sample
E • exceed callbratlon llmlt
B -found In blank
NA -not analyzed
Sep-04 Dec-04 Mar-OS Jun-OS
•
Accutest Laboratories • Report of Analysis Page I of I
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
RWSF-1
Fl6962-6
A Q -Ground Water
SW846 8260B
Project: GELS, Hendersonville, NC
Run#!
Run#2
[Run #1
Run#2
File ID
G0020929.D
Purge Volume
5.0 ml
DF
I
VOA TCL List
CAS No. Compound
7 l--43-2 Benzene
67-66-3 Chloroform
107-06-2 l .2-Dichloroethane
156--59-2 cis-l ,2-Dichloroethylene
156-60-5 trans-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-0l-6 Trichloroethylene
75-01-4 Vinyl chloride
Analyzed By
03/25/03 JG
Result RL
ND ··. 1.0
ND 2.0
ND.>• •2.0
•ND•· . ii2.0
~32<)~-~
J~g /. (~
Date Sampled:
Date Received:
Percent Solids:
03/14/03
03/15/03
n/a
Prep Date
n/a
Prep Batch
n/a
MDL Units Q
0.50 ug/1
0.50 ug/1
0.50 . ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
0.50 ug/1
Analytical Batch
VG727
CAS No. Surrogate Recoveries Run# I Run#2 Limits
1868-53-7
17060-07-0
2037-26-5
460-00-4
Dibromofluoromethane
I ,2-Dichloroethane-D4
Toluene-DB
4-Bromotluorobenzene
110%
115%
97%
. 98% ·
ND = Not detected MDL -Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range
86-115%
78-125%
87-113%
84-117%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evide'O'doij~und O 13
Accutest IaboOUJriP.s •
Client Sample ID:
Lab Sample ID:
Matrix:
RWSF-1
F16962-6
AQ -Ground Water
Report of Analysis
Date Sampled:
Date Received:
Percent Solids:
03/14/03
03/15/03
n/a
Page I of I
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte
Barium
Beryllium
Lead
Manganese
Nickel
Result RL
2s.J'!tT 200
0.26.U 5.0
}OJ . /5.0
12:s::a.. J 15
311 . . 40
RL = Reporting Limit
ID L = Instrument Detection Limit
IDL Units
0.49 ug/1
0.26 ug/1
1.2 ug/1
0.16 ug/1
I.I ug/1
DF
I
I
Prep Analyzed By Method Prep Method
03/20/03 03/21/03 DM SW846 6010B SW846 30lOA
03/20/03 03/21/03 DM SW846 6010B SW846 30lOA
03/20/03 03/21/03 DM SW846 6010B SW846 30lOA
03/20/03 03/21/03 DM SW846 6010B SW846 J0!0A
03/20/03 03/21/03 DM SW846 6010B SW846 J0I0A
U = Indicates a result < ID I() 0 0 0 2 2
B = Indicates a result > = IDL but < RL
020
www.geotra11sinc.com
Dr. Gary Hill
250 Old TyTy Road
Tifton, GA 3 I 794-6607
Reference:
Dear Dr. Hill:
Groundwater Sampling Results
December 2002
GeoTrans Project No. P821-I0I
• I OilO Holcomb Bridge Ro.id
Building I 00, Suite I 'JO
Roswell, GA 30076
770-642-1000 F1\X 770-642-flllOG
February 19, 2003
-' , .. \ ',.
\,,''.
Per your request the results from the recovery and monitoring wells on your property are
provided. The groundwater was analyzed for seven target volatile organic compounds (VOCs),
and five metals. All field and laboratory methods utilized were approved by the U.S.
Environmental Protection Agency (EPA). The results from December 2002 for MW-64, MW-
64A, MW-66 and RWSF-l(see Figure I) are provided in the attached laboratory reports and are
summarized in the attached tables.
EPA requires General Electric to sample the wells quarterly as part of a long-term
monitoring plan. The groundwater will continue to be sampled for seven YOCs, and five metals. The one SVOC, nitrobenzene, has been removed from the quarterly sampling events with EPA
approval. It will be sampled only during the annual sampling events that occur in September of
every year. In the event that nitrobenzene is recovered during the annual sampling event it will be
placed back onto the list for quarterly sampling. We will report groundwater sampling results to
you as they become available. If you have any questions, please feel free to call me at (770) 642-
1000 or Mr. Lee Humphrey at [phone].
cc. Michael Townsend (EPA)
Lee Humphrey (GELS)
David Mattison (NCDENR)
P:IGl:\DOCS\RESIDEN'!\!l ILL RESULTS\liill Results 12-02.wp,J
F~hru>lf)' l'l, 2()()3
Sincerely,
~adl-ilem.1~
Patricia Hermann
Project Scientist
\ \
P:IGE\rgvp\gis-rgvp\SF site. wor
·.·~······,.
,,.,. . .-·
. . .
-·--:-----
·, . ___ j_ __ L
Expla11atio11
• Site monitor well
♦ Recovery well + Sampled Residential well e Piezometer
Q
0
RWSF-2 ♦ ,.._
El
300
SCALE IN FEET
RWSF-3 .. MW-66
··-.. _;·-.
600
RWSF-4'
__ .. ·· \
TITLE:
LOCATION:
~.~ 4Q~
,wz,0~ ~ Bunched':--.. '
arrowh~~~
habitat ---~
BAPZ-7 0
Location of Shepherd Farm Subsite Features
East Flat Rock, NC
~ G o[i DRAFTED PEP ~ e raflS I r---m-,----+-s,-,;,,-.w~---, a ""' ""' """'"' ' nc. DATE 11130/01
CHECKED PAW FIGURE:
1
Table 1. Shepherd Farm Subsite -Perlormance Well Analytical Results.
Remediation MW-64
Parameter Goal Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
voes (µg/L)
1,2-Dichloroethane ND(2.0) ND(2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0)
Benzene Nil ( 1.0) ND (1.0) ND (J.O) ND(JO) ND (JO) ND (JO)
Chlorofom1 1.0 J ND(2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
cis-l ,2-Dichloroethene 70 ND (2.0) ND (2.0) ND(2.Q) ND (2.0) ND (2.0) ND (2.0)
Tetrachloroethene 3.6 2.8 0.83 J 1.9 J 5.0 3.0
trans-1,2-Dichloroethene 70 ND (2.0) ND (2.0) ND(2.0) NO (2.0) ND (2.0) ND (2.0)
Trichloroethene 2.8 ND (2.0) ND (2.0J ND (2.0) ND (2.0) ND (2.0) ND (2.0)
Vinyl chloride ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND ( 1.0) ND (I.OJ
SVOCs (ftg/L)
Nitrobenzene JO ND (5.0) ND(50) ND (5.5) ND (5.0) ND (5.0) ND(5.0)
METALS TOTAL (µg/L)
------------------
l3arium :woo 37.9 H 53 0 J 20.1 J 22.0 J 37.9 J 34.5 J
Beryllium 4 0.68 J 0.68 U 0.51 U 0.75 U 0.67 U 0.451
Lead 15 1.5 J 12.7 3.4 U l.3 U 1.2 U 4.7 U
Manganese ;o 8.4 J 27.7 2.7 UJ 2.7 U 3.4 UJ 7.0 J
Nickd 100 5.4 U 0.8 U !.2 J 0.8 U 0.8 U 0.8 U
Notes: Balded values indicate detected concentrations greater than remediation goals.
U,ND -not detected
J -detected, estimated result
UJ -not detected, estimated result
D -dilution sample
E -exceed calibration limit
B -found in blank
NA -not analyzed
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (JO) ND (1.0) ND (1.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) • ND (2.0) ND (2.0) ND (2.0) ND (2.0)
0.54 J 1.2 J 4.0 ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND(2.0)
ND(2.0) ND (2.0) ND (2.0) ND (2.0)
ND (I.OJ ND (1.0) ND (JO) ND (JO)
NA NA ND (5.0) NA
36.8 J 25.6 J 55.5 J 16.8 J • 0.22 U 0.26 U 0.26 U 0.26 U
8.8 2.8 J 7.9 1.2 U
16.3 J 4.7 J 16.7 6.4 J
1.5 J I.I u I.I u I.I u
. -\ccuu:st LJ.bor:uories • Report of Analysis Poge l of l
Client Sample ID: MW-64
Lab Sample ID: Fl S869-l
AQ • Groumi WJter
SWS-l6 3260B
: .\LHrix:
\ Ylet_hod:
•, Project: GELS. He~decsonvilk. NC
I !Run.:/ I
!Run .;t2
i
!Run 11
iRun .:::
YO . .\. TCL
l.-1.~ '>o.
71--13-2
l"]/-66-J
107-06-2
1 )6-S~-2
I 56-60-5
127-13--l
79-01-6
75-01-...:.
C.-1.S .\o.
1368-53-7
File !D
COU l 3373 D
Pur;;!e V ulume
5.0 ml
Us~
Cumpuund
Be~ze:-:e
C:iioroiorm
DF
1.2-Dicolurnethonc
c,s-l ,2-Dlc!"11orot::f,y;t:nt:
tr:i.'1s-l , 2-D ichlurot:thy lent:
Tetrochloroethylene
T r:c:-lloroethylt:::e
v:,ny\ ch!or;.dt:
Surrogate Recoveries
D: bro mo rl uo romt:ch;.rne
I 7060-IJ7 -0 l .2-Dichloroerh:i.rie•D~
2037-26-5 Tuluene-DS
tl)().1)().-l :L 8 romo t1 L'.Orobe:1zt::1e
RL = Reponin~ LtmH
. .\.nalyzed
l2:'24:02
Result
ND
ND
0iD
.\D
ND
ND
ND
ND
Run#
9 -t7 ) .,
3-Cl.. , ,,
11)7'·.i;
9Y ~T:
E = fmlic.:ict:s ·.-a!•..:c: ,_;:,;:c:::etis ...:J.llbrJliun ri.n~·.:
Bv
JG
RL
1.0
2.0
2.0
2.J
2.0
2.0
2.0
!.O
Run# ' -
Date Sampled: 12/13102
Date Ret:eived: 12/!--L02
Percent Solids: nlo
Prep Date
n.-J.
\ll)L Lnits
0 . .5C ug.:!
0 ,,, ug/!
0 .;;:I,' ug/!
ll.::u ug,ii
I) .::,J ug/!
0.50 ug/1
0 . .5(1 ug/1
0 5(' ug/1
L:mits
3':-\ 15%
-:-! 2:5 r:;,
-1 ! 3 c:;_
't t 7 ~7u
Prep Batch
0/J
Q
j
' ! ) I . ·' I i I ., I . , .,--, I
I
Analytical Batch
VC6IU
] = [r:~:..::.:[~S an i.:slim:.1_ti.:U ·1:ilue . o.oJ,..'1._
1 8 -= {;.,...::·..::.llc:S :.uulyle tounLl 1n :.1.ssoc!:.llt:u mi::huJ r:il:1r./\ , = lc-~:c:Hes presurr.p,i'-e e',llkccc 0t ct curr.p,,unc
001··
OCf'OO'-. ,.. ...,, '-~
.-\..:cutc:st L:.iborJtories • Report of Analysis P:ige l of t
Client Sample ID: MW-64
Lab Sample ID: FI 5869-1
.\(atrix: AQ -Ground Water
Project: GELS. Hendersonville. NC
\letals . .\.nalysis
. .\.nalyte
8:irium
Beryllium
LcaLl
\l:ing:1nc:se
\:,..:'...:::
Result
16.Stl-. I
0.26 l!
l .2 C
6.-lcl--)
I I r· .. :
RL ; Reponing Limi1
RL
200
5.0
5.0
15
-lO
IDL = lnsm.1me:it Dc::e•..:tion Lirn.it
IDL Cnits
0.49 ug/1
0.26 ug/1
1.2 ug..-!
0.16 ug/1
l.l U~:·!
OF
Date Sampled: 12113102
Date Received: 12! l-li02
Percent Solids: n/a
Prep
12119102
12/ l 9/02
l2., l9102
12.119/02
l :. I 01n'"'
Analyzed By
12/20/02
12/20/02
12120102
l 2i20!02
\ :r~o .. ·o:
' I /, ' ,, . I
I
OM
0\1
OM
D\I
D\1
Method
SW3<6 60!0B
SW3<6 60 !OB
S\V3-4o 1J01uB
SWS~o 'JlHOB
S'.V~.lll .,,J'.''•9
L ; lndica1es J result < IDL
Prep 'vlethod
S\V3-L6 30 l0 . .1..
S\V8~o 30l0A
S'.V3.l!i ;ii;v . .:..
sws-.i0 ~1Jt1J.'".
~ '._\'"'..J.1, -.,·,·:1· .. \
B = [rn.!ic:irc:s ::i. result > = IDL bul < RL
Table 1. Shepherd Farm Subsite • Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Benzene
Chlorofonn
cis-1,2-Dichloroethenc 70
Tetrachloroethene
trans-1,2-Dichloroethene 70
Trichloroethene 2.8
Vinyl chloride
SVOCs (µg/L)
Nitrobenzenc 10
METALS TOTAL (11g/L)
Uarium
Beryllium
Load
Manganese
Nickel
Notes;
U,ND. not detected
J -detected, estimated result
UJ -not detected, estimated result
D • dilution sample
E • exceed calibration limit
B -found in blank
NA -not analyzed
2000
4
15
50
100
MW-64A
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0) ND (2.0) ND (2.0J ND (2.0) ND(2.0) ND (2.0J
Nil ( I.OJ Nil (I.OJ ND (1.0) ND(I.OJ ND (I.OJ ND (I.OJ
ND (2.0) ND(2.0) ND (2.0) 0.68 J 0.68 J ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
50.2 46.7 43.1 41.8 42.8 41.8
ND(2.0) ND(2.0) ND (2.0) ND (2.0J ND (2.0) ND (2.0)
ND (2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0J
ND(l.0) ND (1.0) ND (1.0) Nil (I.OJ ND (I.OJ ND (I.OJ
ND (5.0) ND (5.0) ND (5.0J ND(5.0) Nll(5.0J ND (5.0J
34.0 J 33.6 J 36.0 J 32.7 J 29.7 J 30.2 J
0.79 U 0.86 UJ 0.76 U 0.83 U 0.6 U 0.22 U
1.2 U l.7 UJ 2.5 U 1.4U 1.2 J 4.4 U
90.7 76.9 J 92.4 J 70.8 Sl.4J 50.4
1.9 U 0.8 UJ 0.97 J 0.8 U 0.8 U 0.8 U
Boldcd values indica1e detected concentr.itions greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0J ND (2.0J ND (2.0J ND (2.0J
ND {l.O) ND ( 1.0) ND(l.0) ND(I.O)
0.77 J 0.75 J 0.74 J 0.8 J • ND (2.0J ND (2.0J ND (2.0) ND (2.0J
43.8 37.2 36.3 29.5
ND (2.0J ND (2.0J ND (2.0) ND (2.0J
ND (2.0) ND (2.0J ND (2.0J ND (2.0J
ND (I.OJ ND(I.OJ ND (I.OJ ND (I.OJ
NA NA ND (5.0J NA
31.8 J 32.1 J 32.4 J 42.8 J
0.22 U 0.26 U 0.26 U 0.26 U
2.7 J 1.2 u 1.8 U l.2U
54.0 J 93.4 99.5 216
0.8 U I.I u I.I u I. I U
Accutest Laboratories • Report of Analysis Page l of l
\
Client Sample ID:
Lab Sample ID:
Method:
MWMA
Fl5865-I
AQ -Ground Water
SWS46 S2608 I
. Matrix:
Project: GELS. He~dersonvi!!e. NC
Df
Run .#1
Run#:
File ID
BOl3172.D
iRun #I
!Rt.:n /:/'l
Purge Volume
5.0 ml
'
VOA TCL List
C..\S \o.
71-43-2
(J/-66-.3
!07-06-2
l56-j9-2
127-!3--l
79-01-6
75-01-4
Compound
Be:uene
Cilloror'or.n
1.2-Dichlurce•.hane
cis-i .2-Dichloroe~hy\c,e
Tmochloroethv Iese
Tr1chloroerhykne
V'nyl chloride
Surrogc1te Recoveries
1363-53-7 Dibromorluorome:hanc:
'. :060-07 -0 ! . c-D :•c'.:!u rce'.:·.c:r:,-CJ
2037-26-5 Tolue:i.e-D8
!<i0-00-J 4-8 romctl uornbc0.zer.e
RL :;::: R:.:porting Limit
Analyzed
12/23/02
Result
ND
0.30
1'0
'.\D
29 5
ND
ND
Run.4 l
97(:~
91. '·~
98%
1 () \ q.
E :;::: Imiic:ites v::ilue exce..:Us c:i.libr:1~ion rJ.nge
By
JG
RL
1.0
) . _.u
2.0
2.0
2.0
2.0
l.O
Run# 2
Date Sampled: 12/l l/02
Date Received: 12/ 14/02
Percent Solids: n/J
Prep Date
nia
:\-!DL Units
0.50 ug/1
U.5v ug;i
0.50 ug/1
0.50 ugd
-"'\ .::'.1" <J. -,, u;('.
0.50 ug/1
O . .:'O ug/l
0.5C ug/1
l:mits
3-:'-1 l3%
3~-! l I ':T,
Prep Batch
n/a
Q
~ '>-.. .-~j
/
Analytical Batch
VB582
J = [;:C:-::u<.:s .:rn ~sti~Jte·J ••:ilue
8 ~ Inc'•,ares mJ.iyre found in associated me'.hod blank N = rnc:,::1((.:$ presump[ive evidence of ~Qr.'.ROH~d
0 -~ ---~o o 7
Accutest LJbomories • Report of Analy~is Plge l of l
Client Sample ID: MW64A
Lab Sample ID: Fl5865-I
Matrix: AQ · Ground Water
Projct:t: GELS. Hendersonville, NC
Metals .-\nalysis
.-\nalyte Result RL
Bar:um
Beryllium
Lead
MJ.ngmese
Nlckd
< 42.S .\ 200
0.26 U 5.0
I.2 U 5.0
216 I 5
I.I u 40
RL : Reponiw; limit
[DL = lnstr.1rr:e:1t Ot:~e,,:cion Lirr\it
IDL Units
0.49 ug/l
0.26 ug/1
l.2 ug/1
0.16 ug/1
l. l ug/1
DF
Date Sampled:
Date Received:
Percent Solids:
12/ll/02
12/14/02
n/a
Prep Analyzed By c\lethod
t...,,, n I('\..., _, ,.-Iv-l 2!20101 D.\I s·.v:N6 .Jo:os
l 2!19/02 12/20/02 DM SW846 60108
12/l 9/02 I 2/20/02 DM SW846 6010B
l 2!l 9i02 12/20/02 OM SW346 6010B
I 2!! 9102 I 2/20/02 DM SW8466010B
U : !ndicotes a result < IDL
Prep :l,{ethod
s·:,'3~6 ~010 . .\
SW3➔6 2010:\
SIVS46 30 IOA
SW346 3010A
SW3c6 30:0.,
. ' ·i B = fnCicJti.:s::iresult >= !DLbur <:f~L~·.:....-025
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
I ,2+Dichlorocthane
Benzene
Chlorofonn
cis-1,2-Dichloroethene 70
Tetrachloroethene
trans-1,2-Dichloroethene 70
Trichlorot:1hene 2.8
Vinyl chloride
SVOCs (11g/L)
Ni1robenzene 10
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND • not detected
J -detected, estimated result
UJ -not detected, estimated result
0 -dilution sample
E -exceed calibration limit
B -found in blank
NA -not analyzed
2000
4
15
50
100
MW-66
Sep-00 Dec-00 Mar-OJ Jun-OJ Sep-01 Dec-01
ND (2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0)
ND(l.0) ND(l.O) ND (1.0) ND (1.0) ND (1.0) ND (1.0)
ND (2.0) ND (2.0) 0.81 J ND (2.0) 0.77 J ND(2.0)
1.6 J ND (2.0) ND (2.0) ND (2.0) ND(2.0) ND(2.0)
23.2 J 45.8 53.4 54.5 65.7 58.5
ND (2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0)
0.94 J ND (2.0) ND (2.0) ND (2.0) ND(2.0) ND (2.0)
ND (1.0) ND(I.O) ND (1.0) ND ( I.OJ ND (I.OJ ND(I.O)
ND(5.0) ND (5.0) ND (5.5) ND (5.0) ND (5.0J ND (5.0)
52.3 J 36.1 J 39.6 J 26.0 J 40.0 J 39.2 J
1.5 U 0.87 UJ 0.8 U 0.94 U 0.81 U 0.22 U
-1.2 J 1.6 UJ 3.8 U 1.6 U 1.9 J 6.3 U
223 57.3 J 81.2 20.4 119.0 J 98.9
5.3 U 1.8 J 1.8 U 0.8 U 1.2 J 1.9 J
Balded values indicace detected concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND(I.O) ND (1.0) ND (1.0)
0.85 J 0.65 J 0.69 J 0.7 J • ND (2.0) 0.52 J 0.55 J ND (2.0)
61.1 64.8 71.3 76.6
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0J ND (2.0J ND(2.0)
ND ( I.OJ ND(J.O) ND (1.0) ND (1.0)
NA NA ND (5.0J NA
28.0 J 26.5 J 30.8 J 28.9 J • 0.22U 0.26 U 0.26 U 0.26 U
2.5 J 1.2 U 2.5 U 1.2U
16.4 J 25.9 45.0 38.8
0.8 U I.I u I.I u I. I U
Accutest Laboratories •
Report of Analysis Page l or l
Client Sample ID: \!W66
Lab Sample ID: Fl5865-2
Matrix:
Method:
AQ -Ground Water
SW346 32608
Project: GELS, HenJersonviile. NC
Run #l
Run #2
!Run# t
1Run#2
File ID
BOl3l73.D
Purge Volume
5.0 ml
OF
VOA TCL List
CAS 'io. Compound
7l--l3-2 Be'.1.Zer.e
67-66-3 C1loroform
107-06-2 l ,::-DichioroethJ.ne
l56-59-2 c:s-1.2-Dichloroethylene
156-00-5 tr:ins-l ,2-D,chluroethylene
l27-lS-4 Tetr:ichioroethylene
79-01-6 Trichloroethylene
75-0 l --l Vinyl chloride
C.AS :-:o. Surrog:.1£c Recoveries
I S63-5:-7 D iQrorr.o fl uoror.:e~hJ.r.e
l 7060-07-0 l ,2-Dic:1loroe~hJ:1e-D4
2037-26-5 Toluene-OS
4E0-80--1 J. ~ ~(, ....... c ,: , ,,.,.,.,... !-.• --....... ,.
RL ~ R.:porting limit
Analyzed By
l2/23/02 JG
Result
ND
0. 70
ND
ND
ciD
76.6
ND
ND
Run.t l
97%
(,;(J'.,'f V ~ ;(J
l 00% ',~ \ ~-
E = ir.J.icues •11lue c:xc~eds c:illbr.:uion :-::i.r:~':'
RL
! .0
2.0
1.0
2.0
2.0
1.0
2.0
1.0
Run.~ :!.
Date Sampled: 12/10/02
Date Received: l 2/ l .J/02
Percent Solids: n/a
Prep Date
n/a
\IDL Lnits
0 50 mr/l
0.50 ugil
0.50 ug/1
0.50 ug!l
0.5C ug:'I
0.50 ug/1
0.50 ugil
0.50 ug/1
Lmits
26-ll5%
-:, '...,.:::: C7 I·~· 1. _ _, :V
,--I\..., !.-'1 ~ , • 1. 1.) ,U
3.:__ ~ '.: G:
Prep Batch
n/a
Q
I\ .
J
Anal~1ical Batch
VB582
I
8 ~ lnc'cotes anolyte found in J.Ssocioted rr.eua.cd !Jlar~< ~i = [r:C:-::ues oresumotive c•1ic!ence-of--:i/4'.ctr:'PrJUr:d Q Q 8 . . v'-J...J
Accucesc Loborocories • • Report of Analysis
Client Sample ID: ~IW66
Lab Sample ID: F\5865-2
Matrix: AQ -Ground Water
Proje<:t: GELS, Hende,sonvilk, NC
Metals Anal)'Sis
Analyte
B;ir:um
Be,-,;llium
Lead
Mangmese
~i1.J~d
Result
23.9 ~ j
0.26 U
1.2 U
38.3
i. i u
RL = Ri.:por~in~ L!mir
Rl,
200
5.0
5.0
15
~c
IDL = [nsrrnrr.c:1[ Dt~:.:,,.:~ion L:r..ic
IDL Cnits
0.~9 u~:'l
0.26 ug/1
1.2 ug!l
0.16 ug!\
i . l ug;i
OF
Date Sampled: 12110/02
Date Rc>ceived: 12/l4/02
Percent Solids: n/a
Prep Analyzed By Method
t:.'~9/02 :2CO/C2 D'-1 SWSc;.6 ,JO! OB
12/19/02 12/20/02 D~I SW3-+fi 60:0B
12/19/02 12/20/02 DM SW346 60 tOB
12/l 9/02 l 2/20i02 DM SW346 60!0B
12.: l91Ci2 ~2.::~0,02 Q.lv[ S\VS.:.o JIJL0i3
I I ,, I
' ' !
Prep :\lechod
S'iV3~6 1010 . .:..
SW~.J.6 30 ! 0.-\
SW3"6 30 !OA
SW8"6 ,Oto.a
S'.V3'+ci ~OiO.-\
t; = Indicates a resu!c < IDL r. , •i f-'. 8 = 'cdic:ices a cesu!c > = IDL bu~-' QZ6
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/LJ
1,2-Dichloroethane
Benzene
Chlorofonn
cis-1,2-Dichloroethene 70
Tetrachloroethcne
trans-1,2-Dichloroethene 70
Trichlorocchene 2.8
Vinyl chloride
SVOCs (µg/L)
Nitro benzene 10
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND • not detected
J • detected, estimated result
UJ -not detected, estimated result
D -dilution sample
E -exceed calibration limit
B -found in blank
NA· not analyzed
2000
4
15
50
100
RWSF-1
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0) ND(2.0) ND(2.fl) ND(20J ND (2.0) ND (2.0)
ND (1.0) ND(l.O) ND (1.0) ND (1.0) ND (1.0) NO(I.O)
ND (2.0) ND(2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND(:'.0) ND (2.0) ND (2.0) ND (2.0)
34.0 51.4 43.2 0 40.4 46.3 52.6
ND (2.0) ND(2.0) ND(2.Q) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND(2.0) ND (2.0) ND (2.0J ND (2.0) ND (2.0)
ND(l.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND(l.0)
ND (5.0) ND (5.0) ND (5.5J ND (5.5) ND (5.0) ND (5.0J
I 61.0 J 193.0 J 290 242.0 254.0 J 153.0 J
0.3 U 2.6 UJ 2.2 U 2.3 U I.I J 1.2 J
1.5 J 50.6 J 49.5 21.4 24.3 10.4 U
65.6 42.6J l09.0 J l00.0 90.l J 71.8 J
13.7 J 1.4 J 6.5 J 0.8 U 3.5 J 1.8 J
Balded values indicate de1ected concenlrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0J ND (2.0) ND (2.0) ND (2.U)
ND(l.0) ND (1.0) ND (1.0) ND (1.0)
0.52 J ND (2.0J 0.52 J ND.(2.0) • ND (2.0J ND (2.0) ND (2.0) ND (2.0)
56.3 56.4 43.2 63.6
ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0J ND (2.0J ND (2.0)
ND (1.0) ND (I.OJ ND (I.OJ ND (I.OJ
NA NA ND (5.0J NA
156.0 J 142.0J 134.0 J 61.3 J • 0.22 U 0.26 U 0.26 U 0.26 U
26.1 22.7 18.4 l.2 U
98.1 J 105 77.6 0.16 U
4.2 J I.I U I.I U I. I U
Accucest Laboratories • Report of Analysis Page I of l
Client Sample ID: R WSF-l
Lab Sample ID: F\5865-9
Matrix:
Method:
AQ -Ground Water
SW346 32608
Projet:t: GELS, Hendersonville, NC
Run #l
iRunt2
IRunn
Run if2.
File ID
B0l3l75.D
PurJe Volume
5.0 rrJ
OF
I
VOA TCL List
CAS ','o. Compound
71-43-2 Benze:1e
6/-66-3 Ci1ioror"or:n
!07-C6-2 l .2-Dic'.1toroe~hme
156-59-2 cis-i .2-Dic.:hioroethylene
l56-01)-.5 trms-! .2-U itl1iuroeu1 ykne
127-13-4 Tetrachloroethylene
79-0 l-6 Trichioroethylene
75-0 l-4 Vinyl chloride
C.-\S :\o. Sur;-og:...itc R;.;tO\'t:rics
l863-5:-7 D ioromo tluoromethIBe
l 7060-07-0 l ,2-Dichloroe•.har.e-D4
2QJ":'.]~-j T•)l!.:e::t:-0~
-160-00--1 4-8 ro moll uorobenzenc
RL = Rc:;JOr.:in~ Lrr:it
Analyzed By
l2/23/02 JG
Result
"ID
ND
i\D
ND
ND
63.6
ND
ND
R:.m# I
96%
3-v1 I ,o
90~
98%
E = kUic:J.tr:s ·1:ili..:1..; t.:X'..:~.::Js c:1.librJrtor:. r:1n~1~
RL
i.O
2.J
2.0
2.0
:.v
2.0
2.0
LO
Ruitt 2
Date Sampled:
Date Received:
12/l 1/02
12/[4/02
n/a Percent Solids:
Prep Date
n/o
MDL C nits
0 . .:50 ug/1
0.3U ug/1
O.~G ug/1
0.50 un-/1 b"
0.iC ug/1
0.50 ug/1
0.50 ug/1
0 ::;, ..... , .,, ug/!
L;;iits
SG-l 15%
73-125%
~-.: IJctc
3..:.. t17%
Prep Batch
n/a
Q
Analytical Batch
VB582
8 = lr:C:c:Hes :tnJ.lyte four.ct ln :issociared mt:rhot! Jlmk N = [:.1.:.·:::1.res presumptive <;!•1idenc::! of J corr.pou::.d Q 14
Accucest Laboracor.es • Report of Analysis Page l of I
Client Sample ID: RWSF-1
Lab Sample ID: Fl5365-9
~Iatrix: AQ -Ground Water
Project: GELS. Hendersonville, NC
Mecals Analysis
Analyte
Beryllium
Lead
Mar.g:mese
Ni-.:;,>.:t
Resulc
613~
0.26 U
1.2 U
0.16 C
l. l i..:
RL : Rcp,min~ Limit
RL
T 2CO
5.0
5.0
15
-W
IDL -= [nsm.1me:1c De~t·..:tiun L'.1~il
IDL l"nits
0.-19 ug/1
0.26 ug/l
l.2 ug/l
0.16 ug/1
l. l ug/1
OF
Date Sampled: 12/11/02
Date Received: 12/14/02
Percent Solids: n/a
Prep Analyzed By Method
i:n 9102 12/20/02 D~I SW846 60!08
12/19/02 12/20/02 DM SW846 60108
12/19/02 12/20/02 DM SW846 60108
12/19/02 12/20/02 DM SW846 60108
I 2:'I 9/G2 12no,·02 OM S'.V3~6 Qi)1U8
{
l' : Indicates a result < lD L
Prep :Vletbod
SW3~6 !01.0..-\
SW846 J0IOA
SWS-16 3010A
SWS-16 J0IOA
s·.v3~0 jiJ tnA
B : lr.di.c,.tcs a result > = IDL but < RL Q 3 2
,_ ... ,. I.. v,,;_......._0
www.geotransinc.coh1 ,' · . ' '
NOV 1 4 2002
Dr. Gary Hi II
250 Old TyTy Road
Tifton, GA 3 l 794-6607
Reference:
Dear Dr. Hill:
Groundwater Sampling Results
September 2002
Geo Trans Project No. P821-l0 l
I 080 Holcomb Bridge Road
Building 100, Suite 190
Roswell, GA 30076
770-642-1000 FAX [phone]
November 6, 2002
Per your request the results from the recovery and monitoring wells on your property are
provided. The groundwater was analyzed for seven target volatile organic compounds (VOCs),
and five metals. All field and laboratory methods utilized were approved by the U.S.
Environmental Protection Agency (EPA). The results from September 2002 for MW-64, MW-
64A, MW-66 and R WSF-l (see Figure l) are provided in the attached laboratory reports and are
summarized in the attached tables.
EPA requires General Electric to sample the wells quarterly as part of a long-term
monitoring plan. The groundwater will continue to be sampled for seven VOCs, and five metals.
The one SYOC, nitrobenzene, has been removed from the quarterly sampling events with EPA
approval. It will be sampled only during the annual sampling events that occur in September of
every year. In the event that nitrobenzene is recovered during the annual sampling event it will be
placed back onto the list for quarterly sampling. We will report groundwater sampling results to
you as they become available. If you have any questions, please feel free to call me at (770) 642-
lO00 or Mr. Lee Humphrey at [phone].
cc. Giezclle Bennett (EPA)
Lee Humphrey (GELS)
David Mattison (NCDENR)
P:I.GE\DOCS\RES!DENT\HILL Rf:SUL TSII fill R~.sult,OQ.o.!, wr~I
:,.;,,..~mh.:r 6, .!002
Sincerely,
~etdt_ /trk-(aucrL--'
Patricia Hermann
Project Scientist
P:IGElfgvplg1s-rgvp\SFs11e.wor
Exnla11atio11
• Site monitor well
♦ Recovery well .+ Sampled Residential well
0 Piezometer
Q
n
0
0
RWSF-2 ♦
RWSF-~"w"
RWSF-4'
TITLE·
LOCATION:
Location of Shepherd Farm Subsite Features
300 600 1----------------i-::=c----,-=-----~--I -G ri CHECKEDI_PAW~~
East Flat Rock, NC
FIGURE·
SCALE IN FEET
............--.... eo DRAFTED PEP a ◄ 'JfIHAltCHCl'W•~k, rans, Inc. f-F_ll_E __ __,_S_Fs_,te_.w_~ _ _____j
DAlE 11130/01
1
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results.
Remediation
Pa hi meter Goal
-VOCs (g/L)
1,2-Dichloroethane
8cnzene
Chloroform
,.
cis;. 1,2-Dic_hlorocthcnc
Tetrachloroethcnc
..
trans-1-:2-Dichlorocthcnc
.Trichlorocthenc
Vinyl chloride
SVOCs ( g/L)
Nitrobenzcm:
i\lETALS TOTAL ( g/L)
Barium
lkryl)_iu'm
Lead
Manganese,
,1.,:
NiCkcl
Notes:
U,ND -not detected
J • detected, estimated result
UJ -not detected, estimated result
D -dilution sample
I; -excE!ed calibration limit
B -found in blank
70
70
2.8
10
::woo
4
15
50
100
MW-64
Sep-00 Dec-00 Mar-01 J un-0 I Scp-01 Dec-0 I
ND(2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND I 1.0) ND(l.0) ND(l.0) ND ( 1.0) Nil I 1.0) Nll(l.0)
1.0 J ND (2.0) ND (2.0) ND (2.0) ND(2.0) Nil (2.0)
ND (1.0) ND('.!:.<)) ND(1.()) ND(2.0) ND (2.0) Nil (2.0)
3.6 2.8 0.83 J 1.9 J 5.0 3.0
ND(2.0) ND (2.0) ND (2.0) ND (2.0) ND(2.0) ND(2.0)
ND (2.0) ND(2.0) ND (2 0) ND(2.0) ND (2.{l) ND (2.0J
ND(l.0) ND(l.0) ND ( 1.0) ND(l.0) ND (1.0) ND ( 1.0)
ND (5.0) ND (5.0) ND (5.5) ND (5.0) Nil (5.0) ND (5.0)
37.9 ll 53.0J 20. J J ·22.0 J 37.9 J 34.5 J
0.68 J 0.68 U 0.51 U 0.75 U 0.67 U 0.45J
1.5 J 12.7 ).4 u ].) u 1.2 U 4.7 U
84 J 27.7 2.7 UJ 2.7 U J.4 UJ 7.0 J
5.4 U 0.8 U 1.2 J 0.8 U 0.8 U 0.8 U
Ilold,:d values indicate detected concentrations greater than remediation goals.
Mar-02 Jun-02 Scp-02 Uec-02
ND (2.0) ND (2.0) ND (2.0)
ND (1.0) Nil I 1.0) Nil (1.0)
ND (2.0) ND(2.0) ND(2.0) • ND (2.0) ND (2.0) ND (2.0J
0.54 J 1.2 J 4.0
ND (2.0) ND (2.0J ND (2.0)
ND(2.0) ND(2.0) ND (2.0)
Nil (1.0) Nil I 1.0) ND (1.0)
ND(5.0)
)6.8 J 25.6 J 55.5 J • 0.22 U 0.26 U 0.26 U
8.8 2.8 J 7.9
16.J J 4.7 J I 6.7
1.5 J I.I U I. I U
• Accutest Laboratories
Report of Analysis Page l or l
Client Sample ID: MW-64
Lab Sample ID: Fl4503-2
Wlatrix: AQ -Ground Water
Method: SW846 8260B
Project: GELS, Hendersonville, NC
Run #l
Run #2
\Run #l
Run #2
File ID
C00ll85l.D
Purge Volume
5.0 ml
DF
1
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
I 07-06-2 1,2-Dichloroethane
156-59-2 cis-1,2-Dichloroethylene
156-60-5 trans-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-0 l-6 Trichloroethylene
75-0l-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Di bro mo t1 uo romethane
17060-07-0 l ,2-Dichloroethane-D4
2037-26-5 Toluene-DS
460-00-4 4-Bromo fluorobenze:1e
ND = .Not detected
RL = B.cporting Limi_t
Analyzed
09/l9/02
Result
ND
ND
ND
ND
ND
4.0
ND
ND
Run/11
101 %
102%
l0I%
101 %
E = [ndica~es v'1lue ""ceeds calibrat:on range
Date Sampled: 09/10/02
Date Received: 09/l l/02
Percent Solids: n/a
By Prep Date Prep Batch Analytical· Batch
JG n/a n/a VC528
RL Units Q
l.0 ug/1
2.0 ug/1
2.0 ug.'l
2.0 ug/!
2.0 ug/1
2.0 ug/1
2.0 ug/1
1.0 ug/1
Run# 2 Limits
86-115%
78-125%
87-113%
s~-111%
J = fndicates an estimated value ,-. ... , , -
B = [ndicates analyte found in asscdiAtec1-:nB10d biank
N = lr.dicates presumptive evidence of a compound
013
• • Accutest Laboratories
Report of Analysis Page l of l
Client Sample ID: MW-64
Lab Sample ID: Fl4503-2
Matrix: AQ -Ground Water
Method: SW846 8270C SW846 35l0C
Project: GELS, Hendersonville, NC
File ID DF Analyzed
Run #l W0l 1943.D l 09/15/02
Run /12
Initial Volume Final Volume
Run Ill 1000 ml 1.0 ml
Run /12
ABN TCL List
CAS No. Compound
98-95-3 Nitro benzene
CAS No. Surrogate Recoveries
367-12-4 2-Fluorophenol
4165-62-2 Phenol-d5
l 18-79-6 2,-1,6-Tribromophenol
4165-60-0 Nitrobenzene-d5
32 l-60-8 2-Fluorobiphenyl
1718-51-0 Terphenyl-dl4
ND = Not detected
RL = Re?orting Limit
Result
ND
Run# I
43%
30%
79%
66%
64%
85%
E :;;: Indi<;ates value exceeds calib~?tio~ _r,;;mg~
! • . '. !
'.,, -..
Date Sampled: 09/l0/02
Date Received: 09/ l l/02
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
ME 09/12/02 OP5850 SW646
i
'
RL Units Q
5.0 ug/1
Run# 2 Limits
19-90%
10-68%
36-137%
49-119%
45-118%
46-135%
I = Indicates :m estimated value ,~ , ' 7
B = lncicates :malyte found in·associ~(tm'<;,hod bl:mk
N = Indicates presumptive evidence of a compound Q 2 Q
• Accutest Laboratories
Client Sample ID: MW-64
Lab Sample ID: Fl4503-2
Matrix: AQ -Ground Water
Report of Analysis
Date Sampled: 09/10/02
Date Received: 09/11/02
Percent Solids: n/a
Page l of l
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units OF Prep Analyzed By Method Prep 'vlethod
Barium ~h 55.5 B, .' _oo 0.49 ug/1 09/13/02 09/[6/02 OM SW846 60108 S\VS46 3010A
Beryllium 0.26 U 5.0 0.26 ug/l 09/l3/02 09/l6/02 DM SW846 60108 SW846 3010A
Lead 7.9 5.0 1.2 ug/1 09/l3/02 09/ [6/02 DM SW846 60108 SW846 JO lOA
Manganese 16.7 15 0.16 ug/1 09/l3/0: 09/l6/02 DM SW346 60108 SWS-46 JOlO.-\
Nickel 1.1 u 40 l. l ug/1 09/l 3/02 09/16/02 DM SW84660108 SWS46 3010.-\
/ I •-_,
I / ~ .>
RL = Reporting Limit l' = indicates a result < lDLiJ1., ~
ID L = Instrument Detection Limit 8 = indicates a result·->·= -IDL but < RL 0-2 G
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes ( g/L)
1,2-Dichloroethane
lknzene
Chloroform
cis-I ,2-Dichlomethcne
Tetrachloroethene
trans-1,2-Dichloroethene
Trich\orocthene
Vinyl chloride
SVOCs ( g/L)
Nitn?~enzcnc
METALS TOTAL ( g/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:·
U,ND -not detected
J -detected, estimated result
UJ • not detected, estimated result
D • dilution sample
E -exceed calibration limit
.B -found in blank
70
70
2.8
10
2000
4
15
50
100
MW-64A
Sep-00 Dcc-00 Mar-OJ Jun-OJ Sep-0 J Dec-OJ
ND (2.0) Nil (2.0) ND (2.0) Nil (2.0) ND(2.0) ND(2.0)
NDtl.0) Nil (10) ND (10) ND (10) ND ( 10) ND(IO)
Nil (2.0) Nil (2.0) Nil (2.0) 0.68 J 0.68 J Nll(2.0)
ND (2.0) NI> (2.0) Nil (2.0) ND (2.0) ND (2.0) Nil (2.0)
50.2 46.7 43.1 41.8 42.8 41.8
ND (2.0) ND (2.0) Nll(2.0) ND(20) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND(2.0) Nil (2.0)
ND (10) ND ( 10) ND(l.0) Nll(IO) ND(IO) ND (10)
ND (5.0) ND(5.0) ND (5.0) ND (5.0) Nll(5.0) Nll(5.0)
34.0J ]].6 J 36.0 J 32. 7 J 29.7 J 30.2 J
0.79 U 0.86 UJ 0.76 U 0.83 U 0.6 U 0.22 U
1.2 U 1.7 UJ 2.5 U 14 U 1.2 J 4.4 U
90.7 76.9 J 92.4 J 70.8 51.4 J 50.4
19 U 0.8 UJ 0.97 J 0.8 U 0.8 U 0.8 U
Balded values indicate dett:ctcc.J concentralions greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dcc-02
ND (2.0) ND(::U)) ND(2.0)
ND(IO) ND ( IOI ND(IO)
0.77 J 0.75 J 0.74 J
ND (2.0) ND (2.0) ND(2.0) • 43.8 37.2 .16.3
Nil (2.0) ND (2 0) Nil (2.0)
ND (2.0) ND(2.0) ND (2.0J
ND(IO) ND ( 10) ND (10)
Nil (5.0)
l 18 J 32.1 J 32.4 J
0.22 U 0.26 U 0.26 U • 2. 7 J 1.2 u 18 U
54.0J 93.4 99.5
0.8 U 11 U I.I u
• Accutest Laboratories
Report of Analysis Page I of l
Client Sample ID: MW-64A
Lab Sample ID: Fl4503-I
Matrix: AQ -Ground Water
Method: SW846 8260B
Project: GELS, Hendersonville, NC
Run #I
Run #2
!Run #I
Run #2
File ID
C00i 1849.D
Purge Volume
5.0 ml
OF
I
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 l ,2-Dichloroethane
[56-59-2 cis-l, 2-Dichloroethylene
156-60-5 trans-1,2-Dichloroethylene
127-[8-4 Tetrachloroethylene
79-0l-6 Trichloroethylene
75-01-4 Vinyl chloride
CAS No. Surrogate Recoveries
[868-53-7 Dibromofluoromethane
l 7060-07-0 l ,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bro mo fl uo ro benzene
. ND = N.ot detected -
RL = Reporting Limit
Analyzed
09/19/02
Result
ND
0.74
ND
ND
ND
36.3
ND
ND·
Run# 1
100%
102%
103%
105%
. E = Indicates-value t!_xceeds calib-ration· range
~ ,~
'._.'_.)_ '-..£"
--·-
Date Sampled: 09/l0/02
Date Received: 09/11/02
Percent. Solids: n/a
By Prep Date Prep Batch Analytical Batch
JG n/a n/a VC528
RL Units Q
1.0 ug/1
2.0 ug/1 J
2.0 ug/l
2.0 ug/1
2.0 ug/l
2.0 ug/l
2.0 ug/1
1.0 ug/l
Run# Z Limits
86-115%
73-125%
87-113%
34-117%
J = lndic;ues an estimated value
B = lndicites arialvte found in associated n''.~thod blank ·
N = Indicates pres.umptive evidend,J<1t'a'c~p0und
012
• Accutest Laboratories
Report of Analysis Page l of l
Client Sample ID: MW-64A
Lab SampleID: Fl4503-l
MatrLx: AQ -Ground Water
Method: SW846 8270C SW846 35l0C
Project: GELS, Hendersonville, NC
File ID DF Analyzed
Run #l W0l 1942.D l 09/ 15/02
Run #2
Initial Volume Final Volume
Run #l lO00ml l.0 ml
Run.n
ABN TCL List
CAS No. Compound
98-95-3 Ni[robenzene
CAS No. Surrogate Recoveries
367-12-4 2-Fluorophenol
4165-62-2 Phenol-dS
l lS-79-6 2, -l, 6-Tribromophenol
4165-60-0 Nitrobenzene-dS
32 l-60-8 2-Fluorobiphenyl
l7l8-5l-0 Terphenyl-dl4
ND = Not detected ....
RL = Reportin~ Limit ..
Result
ND
Run# l
57%
41 %
89.%
89%
83%
91 % ·
E == Indicates.value exceeds calibration.range .. --[',, :__·, i ,~-:~-
Date Sampled: 09/ l0/02
Date Received: 09/ l l/02
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
ME 09/[2/02 OP5850 SW646
RL l:nits Q
5.0 ug/1
Run# 2 Limits
l9-90%
l0-68 %
36-137%
49-ll9%
45-l 18%
46-135%
J = Indicates an estimated value G··~ i---'t
B = lr.dicates analyte found in associated method blank
N = Indicates presumptive evidence of a compoun(} 1 s ·.
• Accutest Laboratories
Client Sample ID:
Lab Sample ID:
Matrix:
MW-64A
F14503-1
AQ -Ground Water
Report of Analysis
Date Sampled: 09/10/02
Date Received: 09/ l l/02
Percent Solids: n/a
Page I of I
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte
Barium
Beryllium
Lead
Manganese
Nickel
Result
32.4 8
0.26 U
1.s a
99.5
l.l u
RL = Reporting Limit
RL IDL
1100 0.49
5.0 0.26
-::; ' 5.o U I 1.2
15 0.16
40 l.l
IDL = Instrufllent Det,ction Limit
Units
ug/l
ug/l
ug/1
ug/l
ug/1
DF Prep Analyzed By Method Prep :\lethod
09/13/02 09/16/02 DM SW846 60!0B SW846 J0I0A
09/13/02 09/l6/02 DM SW846 60l0B SW846 3010A
09/l3/02 09/ 16/02 DM SW846 60l0B SW846 J0I0A
09/13/02 09/l6/02 DM SW846 60108 SW846 J0!OA
09/13/02 09/16/02 DM SW846 60108 SW846 J0I0A
, i ,} / ' .• 'I.. ' I
, ' d
~---. ' .. ....._
U = Indicates a result< IDLV"-J-J
B = Indicates a result·>= IDL but < RL 025
;1
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes ( g/L)
l ,2-Dichloroethanc
Benzene
Chlorofonn
cis-, l .~;-Dichl?roethene
~",;,.,-'' ,. 1T ctra.c_hloroe1henc
trans-1,2-Dichl~roethcne
Trichloroclhenc
Vinyl chloride
SVOCs ( g/L)
Nitrohcnzcnc
METALS TOTAL ( g/L)
13arium
13cryllium
Lead
Manganese
Nickel
Notes:
U,NO -not detected
J -deteCted, estimated result
UJ 1-not detected, estimated result
D -dilution sample
E -exceed calibration limit
B -found in blank
70
70
2.8
10
2000
4
15
50
100
MW-66
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (20) ND (2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND ( 1.0) ND (10) ND ( 1.0) ND(l.0) Nll(l.0)
ND (2.0) ND (2.0) 0.8 I J ND (2.0J 0. 77 J ND (2.0)
1.6 J ND(2.0J ND (2.0J ND (2.0J ND(2.0) ND (2.0)
23.2 J 45.8 53.4 54.5 65.7 58.5
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND(2.0J
0.94 J ND(2.0) ND(2.0) ND (2.0) ND(2.0) ND (2.0)
ND (1.0) NIJ (1.0) ND ( I.OJ Nll (1.0) ND(l.0) ND(l.0)
ND (5.0) ND (5.0) Nll (5.5) ND (5.0) ND(5.0) Nil (5.0)
52.3 J 36. I J 39.6 J 26.0 J 40.0 J 39.2 J
1.5 u 0.87 UJ 0.8 U 0.94 U 0.81 U 0.22 U
4.2 J 1.6 UJ J.8U 1.6 U 1.9 J 6.3 U
223 57.3 J 81.2 20.4 119.0 J 98.9
5.3 U 1.8 J 1.8 U 0.8 U 1.2 J 1.9 J
13oldcd values indicate detected concentrations greater 1han remediation goals.
Mar-02 Jun-02 Scp-02 Dec-02
ND (2.0) ND (2.0) ND (2.0)
ND ( I.OJ Nll ( 10) ND ( 1.0)
0.85 J 0.65 J 0.69 J
ND (2.0J 0.52 J 0.55 J • 61.1 64.8 71.3
ND (2.0) ND(2.0) ND (2.0)
ND (2.0J ND (2.0) ND(2.0)
ND (1.0) ND (I.OJ ND (1.0)
Nll (5.0)
28.0 J 26.5 J 30.8 J
0.22 U 0.26 U 0.26 U • 2.5 J 1.2 U 2.5 U
16.4 J 25.9 45.0
0.8 U I. I U I. I U
• • Accutest Laboratories
Report of Analysis Page 1 of l
Client Sample ID: MW-66
Lab Sample ID: Fl4503-3
Matrix: AQ -Ground Water
Method: SW846 8260B
Project: GELS, Hendersonville, NC
File ID DF
Run #1 COOi 1852.D 1
Run i/2
!Run #l
Purge Volume
5.0 ml
Run i/2
VOA TCL List
CAS No. Compound
71-43-2 Bem.ene
67-66-3 Chloroform
107-06-2 1.2-Dichioroethane
156-59-2 cis-l ,2-Dichloroethylene
156-60-5 trans-l ,2-Dichloroerhylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Dibromotl uoromethane
17060-07-0 1, 2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromofl uorobenzene
ND ; Not detected
RL = R(:porting Limit
Analyzed
09/19/02
Result
ND
0.69
ND
0.55
ND
71.3
ND
ND
Run# 1
100%
101 %
lOl %
100%
E ; Indicates value exceeds calibration range :
..
Date Sampled: 09/10/02
Date Received: 09/ 11/02
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
JG n/a n/a VC528
RL Units Q
l .O ug/1
2.0 ug/1 J
2.0 ug/1
2.0 ug/1 J
2.0 ug/1
2.0 ug/l
2.0 ug/1
1.0 ug/1
Run# 2 Limits
86-115%
78-125%
87-113%
84-117%
J ; Indicates an estimated value
B ; lnd'cates analyte found in _oss?<;,i",lt;d method blad,
N ; Indicates presumptive evl,i;,n.:e.lof'a compound D 14
Accutest Laboratories • •
Report of Analysis Page I of I
Client Sample ID: MW-66
Lab Sample ID: F14503-3
Matrix: AQ -Ground Water
Method: SW846 8270C SW846 3510C
Project: GELS, Hendersonville, NC
File ID DF Analyzed
Run #I W0I 1969.D I 09/17 /02
Run #2
Initial Volume Final Volume
Run.# I 1000 ml 1.0 ml
Run !/2
ABN TCL List
CAS No. Compound
98-95-3 Nitrobenzene
CAS No. Surrogate Recoveries
367-12-4 2-F!uorophenol
4165-62-2 Phenol-d5
I 18-79-6 2,4,6-Tribromophenol
4165-60-0 Nitrobenzene-d5
321-60-3 2-F!uorobiphenyl
1718-51-0 Terphenyl-d14
ND = Not detected
RL = Reporting Limit_
Result
ND
Run# I
58%
40%
93% .. ·
91 %
87%
93%
E = Indicates value exceeds calibration range
-.
Date Sampled: 09/ 10/02
Date Received: 09/11/02
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
ME 09/12/02 OP5850 SW648
RL Units Q
5.0 ug/l
Run# 2 Limits
19-90%
10-68 %
36-137%
49-119%
45-118%
46-135%
',.
J = Indicates an estimated value
B = Ir.d'cates :malyte found in associated method blank
N = Indicates presumptive evidenc{9(}'.,;l,hlpound O 21
Accutest Laboratories •
Report of Analysis Page l of l
Client Sample ID:
Lab Sample ID:
Matrix:
MW-66
F\4558-1
AQ -Ground Water
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL
30.8'&-; lioo
0.26 U 5.0
IDL
0.49
0.26
Barium
Beryllium
Lead
Manganese
Nickel
2.5 &---/ 5.0 lJ l 1.2
45.0 15 0.16
Ll U 40 1.1
RL = Reporting Limit
IDL = Instrument Detection Limit
Units
ug/l
ug/1
ug/l
ug/1
ug/l
. '
DI'
Date Sampled: 09/10/02
Date Received: 09/12/02
Percent Solids: n/a
Prep
09/ I 7 /02
09/17 /02
09/17/02
09/17/02
09/17/02
Analyzed By
09/18/02
09118/02
09/18/02
09/18/02
09/18/02
' I ;
! /
DM
DM
DM
DM
D~I
Method
SW846 60108
SW846 60108
SIV8>6 60108
SW846 60108
SW846 60108
U = Indicates a result < ID L
Prep :\ lethod
SW846 J0I0A
SW846 3010A
5IV846 J0IOA
SWS>6 3010A
S\V8.t6 3010 . ..\
B = Indicates a result > = IDL but < RL
0-0012 030
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes ( g/L)
1,2-Dichloroethane
lknzcne
Chlornform
cis-1,2-Dichloroethcnc
Tetrachloroethene
trans-1,2-Dichloroethcne
Trichloroethcne
Vinyl chloride
SVOCs ( g/L)
Nitrobcnzenc
~IETALS TOTAL ( g/L)
Barium
Beryllium
Lead
Manganese
Nii.:kel
Notes:
U,NO • not detected
J -detected, estimated result
UJ -not detected, estimated result
D -dilution sample
E -exceed calibration limit
B -found in blank
70
70
2.8
10
2000
4
15
50
JOO
RWSF-1
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0J
ND(I.OJ ND ( 1.0) ND ( 1.0) ND (1.0) Nil (1.0) ND I 1.0)
ND (2.0) ND(::U)) ND(2.0) ND (2.0) ND (2.0) ND(2.0)
ND (2.0) ND (2.0) Nil (2.0) ND (2.0) ND (2.0) ND(2.G)
34.0 51.4 43.2 0 -10.4 46.3 52.6
ND(2.0) ND (2.0) Nll(2.0) Nil (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND(2.0) Nil (2.0)
ND ( 1.0) Nil ( 1.0) ND(l.O) ND (1.0) Nil (I.OJ ND (LO)
ND (5.0) ND (5.0) Nil (5.5) Nil (5.5) ND(5.0) ND (5.0)
161.0 J 193.0 J 290 242.0 254.0 J 153.0 J
0.3 U 2.6 UJ 2.2 U 2.3 U I.I J 1.2 J
1.5 J 50.6 J 49.5 21..t H.3 10.4 U
65.6 42.6 J 109.0 J 1110.0 90.l J 71.8 J
I 3.7 J 1.4 J 6.5 J 0.8 U 3.5 J 1.8 J
Bolded values indicaie dett:cted concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND(2.0) ND(2.0)
Nil (1.0) Nil ( 1.0) ND(l.01
0.52 J ND(2.0) 0.52 J
ND (2.0) ND (2.0) Nil (2.0) • 56.3 56.4 43.2
ND (2 0) ND (2.0) ND (2.0)
ND (2.0) Nll(2.0) Nil (2.0J
ND (1.0) ND ( 1.0) ND ( 1.0)
Nll(5.0J
156 0 J 142.0 J I 34.0 J
0.22 U 0.26 U 0.26 U • 26.\ 22.7 18.4
98.\ J 105 77.6
4.2 J I.I u I. I U
Accutest Laboratories
Report of Analysis Pige l of l
Client Sample ID: RWSF-l
Lab Sample ID: Fl4503-4
Matrix: AQ -Ground Water
Method: SW846 82608
Project: GELS, Hendersonville, NC
Run #l
Run#2
\Run #1
Run i/2
File ID
C00l l853.D
Purge Volume
5.0 ml
OF
I
VOA TCL List
CAS No. Compound
7l-43-2 Benzene
67-66-3 Chloroform
107-06-2 1,2-Dichloroethane
156-59-2 cis-l .2-Dichloroethylene
l56-60-5 trans-1.2-Dichloroethylene
127-l8-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Dibromo fluoromethane
17060-07-0 l ,2-Dichloroethane-D4
:037-26-5 Toluene-D8
460-00-4 4-B romo tl uo ro benzene
ND ; Not detected
RL = Reporting Limit
Analyzed
09/19/02
Result·
ND
0.52
ND
ND
ND
43.2
ND
ND
Run# I
100%
l0l %
l02%
102%
E = f.ndicates value exce::ds calibration range
Date Sampled: 09/ l0/02
Date Received: 09/ l li02
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
JG n/a n/a VC528
RL Units Q
l.0 ug/1
2.0 ug/l J
2.0 ug/1
2.0 ug/1
2.0 ug/1
2.0 ug/l
2.0 ug/1
·1.0 ug/1
Run# 2 Limits
86-l l5%
78-l25 %
87-ll3%
8.!-117%
J ; lndicites an estimated value
B ; Indicates ,nalyte found in .ssociated method blank
N ; Indicates presumptive evidenre-0f•a' iro1nooundD 15 V'\..:_ .........
• Accutest Laboratories
Report of Analysis Page l of I
Client Sample ID: RWSF-1
Lab Sample ID: F 14503-4
Matrix: AQ -Ground Water
Method: SW846 8270C SW846 3510C
Project: GELS, Hendersonville, NC
File ID DF Analyzed
Run #1 W0l 1948.D l 09/16/02
Run #2
Initial Volume Final Volume
Run #I 1000 ml LO ml
Run #2
ABN TCL List
CAS No. Compound
98-95-3 Nitrobenzene
CAS No. Surrogate Recoveries
367-12-4 2-Fluorophenol
4165-62-2 Phenol-d5
118-79-6 2,4,6-Tribromophenol
4165-60-0 Nitrobenzene-d5
321-60-8 2-Fluorobiphenyl
1718-51-0 Terphenyl-dl4
ND = Not detected
RL = Reporting Limit
Result
ND
Run# 1
21%
18%
44%
85%
84%
91 %
E = Indicates value exceeds calibration range
Date Sampled: 09/ 10/02
Date Received: 09/ 11/02
Percent Solids: n/a .. ..
By Prep Date Prep Batch Analytical Batch
ME 09/12/02 OP5850 SW646
I
RL Units Q
5.0 ug/1
Run# 2 Limits
19-90%
10-68%
36-137%
-i9-l 19%
-+5-118%
46-135 %
1 = Indicates an estimated value
B = lr.c,cates analyte found in associated method blank
N = Indicates presumptive evidence of a compoundD? 2
o<:22 -
Accutest Laboratories •
Client Sample ID: RWSF-l
Lab Sample ID: Fl4503-4
Matrix: AQ -Ground Water
Report of Analysis
Date Sampled: 09/10/02
Date Received: 09/1 l/02
Percent Solids: n/a
Page l of l
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units OF Prep Analyzed By Method Prep Method
Barium 134 ~-:boo 0.49 ug/l 09/13/02 09/16/02 OM SW846 60108 SWS46 3010A ·-" Beryllium 0.26 U 5.0 0.26 ug/l I 09/13/02 09/16/02 OM SW846 60108 SW846 30IOA
Lead !8.4 5.0 l.2 ug/l I 09/13/02 09/16/02 OM SW846 60l0B SW846 J0I0A
MJ.nglilese 77.6 15 0.16 ug/l 09/13/0c. 09/16/02 DM SW846 60!08 S\V3-+6 ~O lOA
Nickel l.l u 40 LI ug/1 09/13/02 09/[6/02 OM SW846 60108 SW846 3010A
RL = Reporting Limit U = Indicates a result < !DL
!DL = Instrument Detection Limit 8 = [ndicates a result > = ID L but < RL 027
www.geotronsinc.com
Dr. Gary Hill
250 Old TyTy Road
Tifton, GA 31794-6607
Reference:
Dear Dr. Hill:
Groundwater Sampling Results
June 2002
GeoTrans Project No. P821-101
.0/lO Holcomb Bridge Road
Building I 00, Suite I 'JO
Roswell. Gf\ 30076
770-642-1000 FAX [phone]
August 16, 2002
Per your request the results from the recovery and monitoring wells on your propeny are
provided. The groundwater was analyzed for seven target volatile organic compounds (YOCs),
and five metals. All field and laboratory methods utilized were approved by the U.S.
Environmental Protection Agency (EPA). The results from June 2002 for MW-64, MW-64A,
MW-66 and RWSF-l(see Figure l) are provided in the attached laboratory repons and are
summarized in the attached tables.
EPA requires General Electric to sample the wells quanerly as pan of a long-term
monitoring plan. The groundwater will continue to be sampled for seven YOCs, and five metals.
The one SVOC, nitrobenzene, has been removed from the quancrly sampling events with EPA
approval. It will be sampled only during the annual sampling events that occur in September of
every year. In the event that nitrobenzene is recovered during the annual sampling event it will be
placed back onto the list for quanerly sampling. We will repon groundwater sampling results to
you as they become available. If you have any questions, please feel free to call me at (770) 642-
1000 or Mr. Lee Humphrey at [phone].
cc. Giezelle Bennett (EPA)
Lee Humphrey (GELS)
David Mattison (NCDENR)
P:\GE\DOCS\RESJDENl\tl I LL R F-'iUI. TS\H; 11 Resuh,06-02. •vpd
August 16, 2002
Patricia Hermann
Project Scientist
\SFsi1e WO/ P:\GE\rgvp\gis-rgvp
. · ..
. '_, ....
_·, .·.
. l '
Explanatioll
Site monitor well
: Recovery welldential well + Sampled Rest 0 Piezometer
n
0
g El
RWSF-2 ♦ ,.MW•" RWSF-3
w-.e,
MW-62A •
300
SCALE IN FEET
RWSF-~
0
TITLE: Subsite Features
\; !
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results.
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Benzene
Chlorofonn
cis-1,2-Dichl?~o.ethene 70
Tetrachlorocthene
•trans-1,2-Dichloroethene 70
· · Trichloroethene 2.8
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene 10
METALS TOT AL (11g/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J • detected, estimated result
UJ • not detected, estimated result
D -dilution sample
E -exceed calibration limit
B -found in blank
2000
4
15
50
100
MW-64
Sep-00 Dec-00 Mar-OJ Jun-01 Sep-01 Dec-01
ND (2.0J ND (2.0) ND (2.0J ND (2.0J ND (2.0) ND (2.0J
ND (I.OJ ND(l.OJ ND (I.OJ ND ( I.OJ ND (I.OJ ND(l.OJ
1.0 J ND (2.0) ND (2.0J ND (2.0) ND (2.0) ND (2.0J
ND (2.0J ND (2.0J ND (2.0J ND (2.0J ND (2.0) ND (2.0)
3.6 2.8 0.83 J 1.9 J 5.0 3.0
ND (2.0J ND (2.0J ND (2.0J ND (2.0J ND (2.0) ND (2.0J
ND (2.0J ND (2.0J ND (2.0J ND (2.0J ND (2.0) ND (2.0J
ND (1.0) ND (1.0) ND (I.OJ ND(l.O) ND (1.0) ND (I.OJ
ND (5.0) ND (5.0) ND (5.5) ND (5.0) ND (5.0) ND (5.0J
37.9 U 53.0 J 20.1 J 22.0 J 37.9 J 34.5 J
0.68 J 0.68 U 0.51 U 0.75 U 0.67 U 0.451
1.5 J 12.7 3.4 U 1.3 u 1.2 U 4.7 U
8.4 J 27.7 2.7 UJ 2.7U 3.4 UJ 7.0 J
5.4 U 0.8 U 1.2 J 0.8 U 0.8 U 0.8 U
Boldcd values indicate detected concentrations greater than remediation goals
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND (2.0)
ND (I.OJ ND (I.OJ
ND (2.0) ND (2.0J
ND (2.0J ND (2.0) • 0.54 J 1.2 J
ND (2.0J ND (2.0)
ND (2.0J ND (2.0J
ND (1.0) ND (1.0)
36.8 J 25.6 J
0.22 U 0.26 U • 8.8 2.8 J
16.3 J 4.7 J
1.5 J I. I U
A.ccutesr Laboratories • • Report of Analysis Page l of l
Client Sample ID: MW-64
Lab Sample ID: F 135 l 2-l
Matrix:
Method:
AQ -Ground Water
SW846 82608
Project: GELS. Hendersonville, NC
Run .41
Run4Z
File ID
80010\52.D
Purg:e Volume
5.0 ml
VOA TCL List
C.\S ~o. Compound
71 -..!J-2 Bc::1ze:1.e
57-611-3 Chloroform
DF
l
:0-:--06-2 l ,2-0i~;,toroedur.t::
~56-59-2 ;.;!s-l ,2-Dic!"liorcc:thyie:.1e
t~7-t8-4 Tc:~rachloroe~hyle:-:.e
0 9-01-6 T richloroethy lene
75-01-.l Vinyl chioride
C.-\S ~o. Surro~ate Re<:overies
l 3t8-53-7 Dibromotluoromechane
: i060-U7 -0 l. 2-D ichloroethane-O4
2037-~6-5 Tolue:1c:-D8
C60-iJ0-4 cl-Bromotluorobenzec.e
ND = 'iot detected
RL ::;; Reporring Lim.it
Analyzed
06/\3/02
Result
ND
ND
ND
ND
'.'1D
l.2
ND
ND
Run#
99%
\03%
99%
9fJ %
E ::;; Ir."J.icites valµf ~~C::e:.:!s c::i..!ibr.1do~ :-~g;e
l
By
JG
RL
l.O
2.D
2.-)
2.1J
'\ ,'\
-· ,J
2.0
2.0
l.0
Run# 2
Date Sampled: 06/ l 1/02
Date Received: 06/l 2/02
Percent Solids: n/a
Prep Date
n/a
Cnirs Q
ug/1
ug:l
u; .. l
ug!~ ··~ '1 -=· .
urrl'i , .. J
ug/!
ug,1
Limits
30-120%
30-120%
-~0-i 20%
qrj-l'20%
Prep Batch
n/a
Analytical Batch
VB+l-l
J ::;; fn<lic::ues an .::stim::ited value
B : [r,cicates analyte round ',n. assoc:ated coethod blan.'<
N = rr.c.:cJtes presu.rnptive e·:idc:~C:! of a cam.pound
008
Accutest Laboratories • Report of Analysis Page l of l
Client Sample ID: MW-64
Lab Sample ID: Fl35l2-l
Matrix: AQ -Ground Water
Project: GELS, Hendersonville. NC
Metals Analysis
Analyte
Barium
Beryilium
Lead
:VlangJnese
\icke!
Result RL
25.6&.-1' i 200
0.26 U 5.0
2.8•~ -::r:l. 5.0
4.7B.....71 l5 \.1 V ;_ 40
RL ~ Reeoning Limit
IDL
0..!9
0.26
l.2
0. 16
I. I
IDL = Insuumt=nt Detection Limil
Units OF
ug/1
ug/1
ug/1
ug/1
ug/1
/ / ' . ...,..,,
\; /
(
Date Sampled: 06/l 1/02
Date Received: 06/ l 2/02
Percent Solids: n/a
Prep Analyzed By Method
06il3/02 06/ l4i02 DM SW8<6 60l08
06il3/02 06/14/02 DM SW3<6 GOl08
06il3/02 06/ 14/02 DM SW846 60l08
06/l 3/02 06/ l<!/02 DM SW3-l-6 60l08
06/\3/0: 06/14/02 D~I $\V3-Hi (,0t0B
L ~ indicates a result < lDL
Prep ',,(ethod
S\V3.J.6 30 lOA
SWS<6 30l0A
SW8"'<l 30l0A
SW3<6 :o,o.,
)\V~.:/j ;Ol!l . .l..
B ~ indicates a result > ~ IDL but < RL 016
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Benzene
Chlorofonn
cis-1,2-Dichloroethene
Tetrachloroethene
trans-1,2-Dichloroethene
Trich\oroethene
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene
METALS TOTAL (11g/L)
Barium
Beryllium
L<ad
Manganese
Nickel
Notes:
U,ND -not detected
J -detected, estimated result
UJ • not detected, estimated result
O -dilution sample
E -exceed calibration limit
B -found in blank
70
70
2.8
10
2000
4
15
50
100
MW-64A
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND(LO) ND (LO) ND(LO) ND (LO) ND (LO) ND (LO)
ND (2.0) ND (2.0) ND (2.0) 0.68 J 0.68 J ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
50.2 46.7 43.1 41.8 42.8 41.8
ND (2.0) ND (2.0) ND (2 0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (LO) ND (LO) ND (LO) ND (LO) ND(LO) ND (LO)
ND (5.0) ND (5.0) ND (5.0) ND(5.0) ND (5.0) ND (5.0)
34.0 J 33.6 J 36.0 J 32.7 J 29.7 J 30.2 J
0.79 U 0.86 UJ 0.76 U 0.83 U 0.6 U 0.22 U
1.2 u 1.7 UJ 2.5 U l.4U 1.2 J 4.4 U
90.7 76.9 J 92.4 J 70.8 51.4 J 50.4
L9 U 0.8 UJ 0.97 J 0.8 U 0.8 U 0.8 U
Bolded values indicate detected concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND (2.0)
ND (LO) ND (LO)
0.77 J 0.75 J
ND (2.0) ND (2.0) • 43.8 37.2
ND (2.0) ND (2.0)
ND (2.0) ND (2.0)
ND (LO) ND (LO)
3 L8 J 32. I J
0.22 U 0.26 U • 2.7 J 1.2 u
54.0 J 93.4
0.8 U LIU
Accutest Laboratories • • Report of Analysis P:ige l or" l
Client Sample ID: MW-64A
Lab Sample ID: Fl35l2-2
Matrix:
Method:
AQ · Ground Water
SW846 82608
Project: GELS, Hendersonville, NC
Run #l
Run /f2
iRun .11
1Run /12
File ID
80010153.D
Purge Volume
5.0 ml
DF
VOA TCL List
CAS 'lo. Compound
71--13-2 Bc::1.zene
67-,S6-3 C:1loror'om1
[07-06-2 l .2-Dic:iloroetbane
[56-59-2 cis-;. ,2-Dichloroe[hylene
[5o-o0-.i tra.ns-l, 2-0 icaloroerhy ienc:
127-18-.J Te,rachloroethyle:ie
79-01-6 Trichloroethylene
75-0 l--l Vinyl chloride
C.-1.S :-lo. Surrogate Recoveries
l 868-53-7 D lbromo t1uororr.elhane
l 7060-07 .() l ,2-Dichloroethane-D4
2037<Z6-5 Tolueoe-D8
-160-1)0--1 4-3romo r1uorohtnze:1t::
:S.D ~ Not detected
RL = Reporting Limit
Analyzed
06/13/02
Result
ND
0.75
ND
ND
ND ... ~} .;,,,_
ND
ND
Run# 1
102%
105%
99%
96 ~Ti
E = lndicait:s ·,alue c:xc::eds cJ.iibration range
By
JG
RL
LO
2.0
:.o
2.0
2.0
2.0
2.0
l.O
Run/I 2
Date Sampled: 06/1 l/02
Date Received: 06il2/02
Percent Solids: n/o
Prep Date
n/a
C nits Q
ug:"l
:12:/l J
uo-n O"
ug:l
ug. l
ug:'l
ug/1
ug/!
Limits
3G-l20%
30-[20%
38-120%
-3C·-l20%
Prep Batch
n/o
Analytical Batch
VB-W.J
1 = 1nd:c::ues m estimated value
B ~ Indicates analyte found in associated :nelhod blank
N = Ir.dicates presumptive evidence of a compound Q Q 9 ~
.. _:._, u ~
Accutt:St LaborJtorit:s • • Report of 1-\.nalysis
Client Sample ID: 1!W-64A
Lab Sample ID: Fl3512-2
Matri:c AQ -Ground Water
Project: GELS. Hendersonville. NC
Metals Analysis
Analyte Result RL
Barium
Bery Iii um
Lead
32 l 'fl..._°3 \ 200
M :lI1 g:J.I1ese
:-iic!<d
0.26 U
l.2 U
93.4
t.~ C
RL ::::: Reportin~ Limit
5.0
5.0
15
~()
ID L = Instrument Detection Limit
IDL Units
0.49 ugil
0.26 ug!l
1.2 ug/1
0. [6 ug/l
l.l u (l" /1 ~ ..
DF
Date Sampled: 06/ l l /02
Date Received: 06/l2/02
Percent Solids: nfa
Prep Analyzed By Method
061 l3,02 06/l4/02 DM SW8>6 60108
06il3/02 06/l4/02 DM SW346 60108
06/ [3102 06il4/02 DM SW846 60108
06/13/02 06/ 14102 DM SWS46 60108
06/ 13.iC: ()6/ l-l/02 D\l SW~J.fi ·i01O9
I , I r,,-/ !_.//1-)
. / / l./ , ·, I 1 _,.
,I f
U = lndicates a result < IDL
Prep :\!ethod
SWS06 JOIOA
SW3>6 JOIOA
SW3-l.6 30!0..\
SW3<6 JO 10.\
S\\'3..!6 2C• '.1; .~.
B = lndicares a result->= IDLbut < RL 017-: ·
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Benzene
Chlorofonn
cis-1,2-Dichloroethene
Tctrachlorocthene
trans-1,2-Dichlorocthene
Trichlorocthene
Vinyl chloride
SVOCs (µg/L)
Nitrobcnzene
METALS TOT AL (11g/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J -detected, estimated result
UJ -not detected, estimated result
D • dilution sample
E • exceed calibration limit
B -found in blank
70
70
2.8
10
2000
4
15
50
100
MW-66
Sep-00 Dec-00 Mar-0I Jun-0I Sep-0I Dec-0I
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND ( 1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0)
ND (2.0) ND (2.0) 0.81 J ND (2.0) 0.77 J ND (2.0)
1.6 J ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
23.2 J 45.8 SH 54.5 65.7 58.5
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
0.94 J ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND(l.0) ND (1.0) ND (1.0) ND (1.0)
ND (5.0) ND (5.0) ND (5.5) ND (5.0) ND (5.0) ND (5.0)
52.3 J 36. I J 39.6 J 26 0 J 40.0 J 39.2 J
1.5 U 0.87 UJ 0.8 U 0.94 U 0.81 U 0.22 U
4.2 J 1.6 UJ 3.8 U 1.6 U \.9 J 6.3 U
223 57.3 J 81.2 20.4 119.0J 98.9
5.3 U \.8 J \.8 U 0.8 U 1.2 J 1.9 J
Balded v::ilucs Indicate de1cc1ed concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND (2.0)
ND (1.0) ND (1.0)
0.85 J 0.65 J
ND (2.0) 0.52 J • 6 \.I 64.8
ND (2.0) ND (2.0)
ND (2.0) ND (2.0)
ND (1.0) ND (1.0)
28.0 J 26.5 J
0.22 U 0.26 U • 2.5 J l.2U
16.4 J 25.9
0.8 U I.JU
Accutest L:iboratories • Report of Analysis Page l of 1
Client Sample ID: MW-66
Lab Sample ID: 1'13512-4
~latri.x:
Method:
AQ -Ground Water
SW846 8260B
Project: GELS, Hendersonville, NC
Run.¥ I
Run .12
File ID
B0010155 D
Purge Volume
5.0 ml
DF
VO..\ TCL Lst
C..\S 'io. Compound
71--13-1 Be:izene
,,---'56-3 C:1iorofor.-:-i
107-06-2 l .2-Dichloroechane
156-59-2 cis-1.2-Dic~lorot:thykm:
156-60-5 tr:ms-l ,2-Dichloroeth ylene
127-18-4 T elr:ic!J.l o roe thy lene
79-0 l -6 Trichloroethylene
75-0 l-4 Vinyl chloride
C.-1.S :-,;o. Surrogate Recoveries
1368-51-7 D ibromor1uoromethane
17060-07-0 l. 2-D ichloroerh:me-D4
2037-26-5 Toiuene-D8
-160-00-.J 4-arorr:o rl uorohenzene
ND = Not derected
RL = Reponing Limit
Analyzed
06/ 13/02
Result
ND
() liS
ND
0.52
ND
64.3
ND
ND
Runil I
99%
l02%
99%
94 si
E = lndic?tes ·,alut: cxc.::~ds ca.libr~uion range
By
JG
RL
'.')
2. ')
2 ,J
2.1)
2.J
2.0
2.()
l.0
Run# 2
Date Sampled:
Date Received:
06111/02
06112/02
n/a Percent Solids:
Prep Date
n/o
Units Q
u 'Z.' '.
'_!~ •
ug.1:
ug:·'. I
ug.,i
ug.-'!
ug:l
uo_;I -'
Limits
30-120%
30-i.20%
~0-120 :-u
30-tlO~t
Prep Batch
n/a
Anal~~ical Batch I
VB44-l
J = Ir!dic::aes J.Il estimated value
B = [~dic:ites analyte found in associated mt:thod blank
N = Ir:c!ic:ites presumptive (!vidence of_J. compound O 11 ...
1 .
A.:cutt!st Labora.torit:s • Report of Analysis Page l of l
Client Sample ID: MW-66
Lab Sample ID: FIJ5 l2-4
Matrix: AQ -Ground Water
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL
Barium
Beryllium
Lead
Manganese
~,.l(.~'\.d
26 5 'l(J r 200
0.26 U 5.0
l.1 U 5.0
25.9 15
l 1 1' '' u ~o
RL = Re;,oni□

g

Limit
IDL
0.49
0.26
1.2
0.16
Li
IDL = Instrument Dece<::ion Limit
Units
ug/l
ug/l
ug/l
ug/l ., ug:1
OF
l
l
I
Date Sampled: 06/ l l/02
Date Received: 06/ 12/02
Percent Solids: n/a
Prep Analyzed By Method
06/1 J/02 06114/02 DM SW841i 60108
06/ lJ/02 06/ 14/02 DM sws.;; 60100
06113/02 06/ 14/02 DM SW846 60108
06/13/02 06114/02 DM SWS4660108
06,.1Ji"0: 06/ l-+/02 DM S\.VS-+<i VOiOB
C = [ndicates a result < IDL
Prep y{etbod
SW846 J0I0A
SW346 J0I0A
SW8•6 J0I0A
SW346 J0ID,\
S\v5..:.11 30 :c,..:..
8 = Indicates a result > = IDL but < RL 019
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Benzene
Ch\orofonn
cis-1,2-Dich\orocthene
Tctrachloroethene
trans-1,2-Dichloroethene
Trichloroethene
Vinyl chloride
SVOCs (µg/L)
Nitro benzene
METALS TOTAL (I1g/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J • detected, estimated result
UJ -not detected, estimated result
D • dilution sample
E • exceed calibration limit
B -found in blank
70
70
2.8
ID
2000
4
15
50
100
RWSF-1
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND(l.0) ND(l.0) ND(l.0) ND(l.O) ND (1.0) ND (1.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
34.0 51.4 43.2 0 40.4 46.3 52.6
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (I.OJ
ND (5.0) ND (5.0) ND (5.5) ND (5.5) ND (5.0) ND (5.0)
161.0 J I 93.0 J 290 242.0 254.0 J 153.0 J
0.3 U 2.6 UJ 2.2 U 2.3 U I.I J 1.2 J
l.5J 50.6 J 49.5 21.4 2-1.3 10.4 U
65.6 42.6 J 109.0J 100.0 90.1 J 71.8 J
13.7 J 1.4 J 6.5 J 0.8 U 3.5 J 1.8 J
Balded values indicate detected concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0) ND (2.0)
ND (1.0) ND (1.0)
0.52 J ND (2.0)
ND (2.0) ND (2.0) • 56.3 56.4
ND (2.0) ND (2.0)
ND (2.0) ND (2.0)
ND ( 1.0) ND (1.0)
156.0 J 142.0 J
0.22 U 0.26 U
26.1 22.7
98.1 J 105
4.2 J I.JU
Accutest Laboratories • • Report of Analysis P1ge l of l
Client Sample ID: RWSF-1
Lab Sample ID: Fl35l2-3
Matrix:
Method:
AQ -Ground Water
SW846 8260B
Project: GELS. Hendersonville. NC
Run #I
Run #2
I
iRun ;/ l
iRun /;?.
File ID
B0010154.D
Purge Volume
5.0 ml
OF
VOA TCL List
C.-1.S 'io. Compound
7 !-43-2 Benzene
67-,S6-3 Chloroform
l O, .,)6-2 l ,2-Dichlorot:thant:
156-59-2 cis-i ,2-Dichloroethylene
Ljti-v0-j ffaILS-l ,2-DiL:hloroethylene
127-13--+ Tetr1chloroethyle□e
79-0 l-6 T richloroethy lene
75-01-4 Vinyl chloride
CAS :-lo. Surrogate Recoveries
· 1363~5~-7 D1bromo rl uoromeL11ne
l c060-07-0 l .2-DichloroeL11ne-D4
2037-?.6-5 Toluece-D8
-\60-•l0-~ ~-3romu r1uorobe1rene
ND = Not uetecced
RL = Reporting Limit
Analyzed By
06/\3/02 JG
Result
ND
ND
ND
ND
ND
56.-l
ND
ND
Run# l
98%
103%
98%
91\'fa
E :;::; IndicJ.tes ·,aJ.ue c::cceeds calibration rangt:
RL
l.O
2.0
2.0
2.0
2.0
2.0
2.0
1.0
Run# 2
Date Sampled: 06/l 1/02
Date Received: 06112/02
Percent Solids: n/a
!_'rep Date
n/a
Cnits Q
ug.-1
u~ !
ug:l
ug:l
ug:1
ug:!
ug/1
ug:l
Limits
30-120%
.30-1:!0%
.30-120%
:-'.O-l20%
Prep Batch
n/a
Analytical Batch
VB444
J = lndic:nes 1n estimated nlue
B = /r.dic1tes malyte found in ,ssociated meL'iou bla.nk
N :;::; I.ndicates presumptive evidt:m.:e or· a compound Q 1 Q
,. ..:..J
Accutest Laboratories • Report of Analysis Pagelofl
Client Sample ID: RWSF-1
Lab Sample ID: F\3512-3
Matrix: AQ -Ground Water
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units
Barium l42B. j j 200 0.49 ug/1
Ber1llium 0.26 U' 5.0 0.26 ugil
Lead 22.7 5.0 1.2 ug!l
Manganese 105 l5 0.16 ug/l
Nickel l.l u 40 l. l ug/1
RL = Reponing limit
ro L = Insrrument Detection Limil
OF
Date Sampled: 061 l l/02
Date Received: 06i l 2/02
Percent Solids: n/a
Prep Analyzed By Method
06/ lJ/02 06/14/02 DM SW846 (1010B
06/l3/02 06/14/02 DM SW846 60l08
06il3/02 06/14/02 DM SW846 tiDlOB
06il 3/02 06/ H/02 DM SWS46 6010B
06il3/02 06i 14/02 DM SW846 60108
I .,, v/jz 1/1/' 7')_ I U: i ' ,/
U = Indicates a result < ID L
Prep \lethod
SW8>6 20l0.-\
SWS..J.6 .;o !fl.-\
S\VS~6 20 ~U.;
SW8-!6 .;Q lO.-l:.
SW346 2010.-\
B = [ndicares a result > = ID L bur 5 R L :fil8
www.geotransinc.com
Dr. Gary Hill
250 Old TyTy Road
Tifton, GA 31794-6607
Reference:
Dear Dr. Hill:
Groundwater Sampling Results
March 2002
GeoTrans Project No. P821-101
.080 H_olcornb Bridge Road
Builcl1ng I 00, Suite 190
Roswell, GA 30076
770-642-1000 FAX [phone]
May 28, 2002
I (.. . .,_
\ J
Per your request the results from the recovery and monitoring wells on your property are
provided. The groundwater was analyzed for seven target volatile organic compounds (VOCs),
and five metals. All field and laboratory methods utilized were approved by the U.S.
Environmental Protection Agency (EPA). The results from March 2002 for MW-64, MW-64A,
MW-66 and RWSF-l(sce Figure I) are provided in the attached laboratory reports and are
summarized in the attached tables.
EPA requires General Electric to sample the wells quarterly as pa1t of a long-term
monitoring plan. The groundwater will continue to be sampled for seven VOCs, and five metals.
The one SVOC, nitrobenzene, has been removed from the quarterly sampling events with EPA
approval. It will be sampled only during the annual sampling events that occur in September of
every year. ln the event that nitrobenzene is recovered during the annual sampling event it will be
placed back onto the list for quarterly sampling. We will report groundwater sampling results to
you as they become available. If you have any questions, please feel free to call me at (770) 642-
1000 or Mr. Lee Humphrey at [phone].
cc. Giezelle Bennett (EPA)
Lee Humphrey (GELS)
David Mattison (NCDENR)
P:IGE\DOCS\RESIDENl\1111.L RESULTS\llill Rc~ult,.03-02. wpd
,\1:.,.y ~8. 2002
Sincerely,
~C(d-4rMCUdl./
Patricia Hermann
Project Scientist
P:IGElfgvp\gis-rgvp\SFsite.wor
' ' --:--~ -----
Explanation
• Site monitor well
♦ Recovery well
~· Sampled Residential well
0 Piezometer
RWSF-2 ♦ ·
RWSF-3 .. "W•"
0.·
. ----
/ ;;•··
/_-., /{,:
MW-61
0
' '
;
I
300
' ,
I !
SCALE IN FEET
RWSF-4'
TITLE:
Location of Shepherd Farm Subsite Features
LOCATION: East Flat Rock, NC
600 CHECKED PAW ~ G OT DRAFTED PEP a ,,.,. rH~•
1
~
0
.. ~} Ir ans, Inc. "',-IL-E--1-s-,-,.,-.-.,-,--1
DA TE 11/30/01
FIGURE:
1
Table D-2. Shepherd Farm Subsite • Performance Well Analytical Results.
Remediation
Parameter Coal
voes (µg/L)
1,2-Dichloroethane
Benzene
Chlorofonn
cis-1,2-Dichloroethene 70
Tetrachloroethene
1rans-l ,2-Dichloroethene 70
Trichloroethene 2.8
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene JO
METALS TOTAL (11g/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J -detected, estimated result
UJ • not detected, estimated result
D • dilution sample
E • exceed calibration limit
B -found in blank
2000
4
15
50
JOO
MW-64
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND(l.O) ND (I.OJ ND(I.OJ
1.0 J ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0J ND (2.0) ND (2.0) ND (2.0)
3.6 2.8 0.83 J 1.9 J s.o 3.0
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2 0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND ( 1.0) ND (1.0) ND ( 1.0) ND (1.0) ND ( 1.0)
ND (5.0) ND(5.0) ND (5.5) ND (5.0) ND (5.0) ND (5.0)
37.9 B 53.0 J 20.1 J 22.0 J 37.9 J 34.5 J
0.68 J 0.68 U 0.51 U 0.75 U 0.67 U 0.451
1.5 J 12.7 HU 1.3 u 1.2 U 4.7 U
8.-1 J 27.7 2.7 UJ 2.7 U 3.4 UJ 7.0 J
5.4 U 0.8 U 1.2 J 0.8 U 0.8 U 0.8 U
Bolded values indicate detected concentrations greater than remediation goals.
l\lar-02 Jun-02 Sep-02 Dec-02
ND (2.0)
ND (I.OJ
ND (2.0)
ND (2.0) • 0.54 J
ND (2.0)
ND (2.0)
ND (I.OJ
36.8 J
0.22 U
8.8
16.3 J
1.5 J
Accutest L!bomories •
Report of Analysis P,ge \ of \
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
MW-64
Fl2586-2
AQ -Ground Water
SW846 8:0608
Project: GELS, Hendersonville, NC
Run .#1
Run#2
File ID
C0008832.D
VOA TCL List
DF Analyzed By
03/15/02 JG
CAS c'lo. Compound Result RL
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 l .2-Dicbloroethane
156-59-2 cis-l ,2-Dichloroethylene
156-60-5 trons-l ,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-0 l-6 Tricbloroethylene
75-0 l-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
l 7060-07-0 l ,2-Dicbloroethone-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromofluorobenzene
ND = Not detected
RL = Reporting Limit
ND
ND
ND
ND
ND
0.54
ND
ND
Run# 1
-104%
·104%
98%
98%
E = [ndicates value exceeds calibration rouge
l.0
2.0
2.0
2.0
2.0
2.0
2.0
l.0
Run# 2
Date Sampled:
Date Received:
03/ [2/02
03/\3/02
n/1 Percent Solids:
Prep Date
n/a
units Q
ug.:l
ug:'l
ugil
ug:l
ugd
ug:'l J
ucr,\ ~"
ug:'l
Limits
30-120%
80-120%
30-120%
30-120%
Prep Batch
n/a
Analytical Batch
VC-l04
I = lndicates m estimated value
B = lndicates malyte found in associated method blar-~
N '= Lndicates presumptive t:vidence of a comgt)un_d.; :~ U!_'on'9
Accutest La.boratories
Client Sample ID:
Lab Sample ID:
Matrix:
MW-64
Fl2586-2
•
AQ -Ground Water
• Report of Analysis
Date Sampled: 03112/02
Date Received: 03/13/02
Percent Solids: n/ a
Page l of l
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units DF Prep Analyzed By Method Prep \lerbod
Barium 36.3 ~ 1.aoo 0.94 ug/1 03/14/02 03/15/02 DM SW846 6010B SW846 J0I0A
Beryllium 0.22 U. 5.0 0.22 ug/1 I 03/14/02 03/ 15/02 DM SW846 6010B SW84<i 3010A
Lead 8.3 5.0 1.2 ug/1 I 03/14/02 03/ 15/02 OM SW846 6010B SW846 30 I0A
Manganese 16.3 '"! I 15 0.26 ug/1 03/14/02 03/15/02 OM SW846 6010B SW846 J0I0A
Nickel 1.5 e-..._'1'L 40 0.30 ug/1 03/ 14/02 03/ 15/02 OM SWS-16 60l0B SW84<i J0I0A
RL = Reponing Limit l = Indicates a result < IDL
ID L = lnstrument Detection Limit B = Indicates a result > = ID L but < R4:i ," i ~ u .,01-s
Table D-2. Shepherd Farm Subsite • Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Benzene
Ch\orofonn
cis-1,2-Dichloroethcne 70
Tetrachloroethene
trnns-I ,2-Dichloroethenc 70
Trichloroethene 2.8
Vinyl chloride
SVOCs (µg/L)
Nitrobenzi:ne 10
METALS TOTAL (ltg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,NO -not detected
J -detected, estimated result
UJ • not delected, estimated result
D • dilution sample
E -exceed calibration limit
B -found in blank
2000
4
15
50
100
MW-64A
Sep-00 Dcc-00 Mar-01 Jun-01 Sep-01 Dec-01
ND(2.0) ND (2.0) ND (2.0) ND(2.Q) ND (2.0) ND (2.0)
ND (LO) ND (1.0) ND ( 1.0) ND (1.0) ND (1.0) ND (1.0)
ND (2.0) ND (2.0) ND (2.0) 0.68 J 0.68 J ND (2.0)
ND (2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0)
50.2 46.7 43.1 41.8 42.8 41.8
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND ( 1.0) ND ( 1.0) ND ( 1.0) ND (1.0) ND ( 1.0) ND (1.0)
ND(5.0) ND (5.0) ND (5.0) ND (5.0) ND (5.0) ND (5.0)
34.0 J 33.6 J 36.0 J 32. 7 J 29.7 J 30.2 J
0.79 U 0.86 UJ 0.76 U 0.83 U 0.6 U 0.22 U
1.2 U 1.7 lJJ 2.5 U 1.4 U 1.2 J 4.4U
90.7 76.9 J 92.4 J 70.8 51.4 J SOA
1.9 U 0.8 UJ 0.97 J 0.8 U 0.8 U 0.8 U
Balded values indicate detected concentrations greatt:r than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0)
ND (1.0)
0.77 J
ND (2.0) • 43.8
ND (2.0)
ND (2.0)
ND (I.OJ
31.8 J
0.22 U
2.7 J •
54.0 J
0.8 U
Accutest Liboratories •
Report of Analysis Page l of l
Client Sample ID: MW-64A
Lab Sample ID: Fl2586-l
Matrix: AQ -Ground Water
Method: SW8-l6 3260B
Project: GELS, Hendersonville, NC
File ID DF
Run .~l C000883 l.D l
Run #2
VOA TCL List
CAS No. Compound
7l-43-2 Benzene
67-66-3 Chlorofonn
107-06-2 1,2-Dichloroethane
[56-59-2 cis-1,2-Dichloroethylene
156-60-5 trans-1,2-Dichloroethylene
127-13-.\ Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-.\ Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
17060-07-0 1,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-.\ 4-Bromofluorobenzene
ND = Not detected
RL = Reponing Limit
Analyzed
03115102
Result
ND
0.77
ND
ND
ND
43.8
ND
ND
Run# l
104% .•..
.105%
99%
99%
E = [ndicates value exceeds calibration range
By
JG
RL
1.0
2.0
2.0
2.0
2.0
2.0
2.0
1.0
Run# 2
Date Sampled: 03/ l 2/02
Date Received: 03/l3/02
Percent Solids: n/a
Prep Date Prep Batch Analytical Batch
nla n/a VC.\04
Units Q
ugfl
ug/1 J
ug,1l
ug/l
uo,:1 ~--
uod ~·· ucr ;1 ~--
ug/l
Limits
30-l20%
80-120%
80-120%
80-120%
J = Indicates an estimated value
B = [ndicates analyte found in associated method blank
N = L1dicates presumptive evidence of a CD'lJP,Wnd " r,,, l ·· _, ~oos
Accutest Libor:llories • Report of Analysis Page I of I
Client Sample ID:
Lab Sample ID:
Matrix:
MW-64A
Fl2586-l
AQ -Ground Water
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte
Barium
Beryllium
Lead
Manganese
Nickel
Result RL
318 ~ "12200
0.22 u .· i;·o
2.7~-r .0
54.0 'l" l 15
0.80 U 40
RL = Reporting Llffiit
IDL
0.94
0.22
1.2
0.26
0.80
ID L = lnstrument Detection Limit
Units
ug/l
ug/1
ug/1
ug/1
ug/1
DF
l
l
Date Sampled:
Date Received:
Percent Solids:
03/12/02
03113/02
n/a
Prep Analyzed By Method
03/14/02 03/15/02 OM SW846 6010B
03/14/02 03/15/02 OM SWS46 6010B
03/14/02 03/15/02 OM SWS46 6010B
03/[4/02 03/15/02 OM SWS46 6010B
03/14/02 03/15/02 DM SW846 6010B
Prep :1-lethod
SWS46 JOIO.-\
SWS46 ,010.-\
SWS46 JO\U.-\
SWS46 JO l0.-\
SW846 JOIO.-\
U = Indicates a result < ID L
B = Indicates a result > = IDL but {R].1 ?
017
Table D-2. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Benzene
Ch!orofonn
cis-1,2-Dichloroethene 70
Tetrach!oroethene
trans-1,2-Dichloroethene 70
Trichlorocthcnc: 2.8
Vinyl chloride
SVOCs (µg/L)
Nitro benzene 10
METALS TOTAL (11g/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J -detected, estimated result
UJ -not detected, estimated result
D -dilution sample
E -exceed calibration limit
B •found in blank
2000
4
15
50
100
MW-66
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0J ND (2.0J ND(2.0) ND (2.0J ND (2.0J ND(2.0)
ND (1.0) ND (1.0l ND (I.OJ ND (I.OJ ND (1.0) ND ( I.OJ
ND (2.0J ND(2.0) 0.81 J ND (2.0) 0.77 J ND (2.0J
1.6 J ND (2.0J ND(2.0) ND (2.0J ND (2.0) Nil (2 OJ
23.2 J 45.8 53.4 54.5 65.7 58.S
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
0.94 J ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND(2.0J
ND(l.OJ ND(l.O) ND(l.O) ND (I.OJ ND (I.OJ ND(l.O)
ND (5.0) ND(5.0J ND (5.5J ND (5.0J ND (5.0J ND(5.0J
52.3 J 36.1 J 39.6 J 26.0 J 40.0 J 39.2 J
1.5 u 0.87 UJ 0.8 U 0.94 U 0.81 U 0.22 U
4.2 J 1.6 VJ 3.8 U 1.6 U 1.9 J 6.3 U
223 57.3 J 81.2 20.4 119.0 J 98.9
5.3 U 1.8 J 1.8 U 0.8 U 1.2 J 1.9 J
Balded values indicate detected concenirations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND(2.0J
ND (J.O)
0.85 J
ND (2.0) • 61.1
ND (2.0J
ND (2.0)
ND(l.OJ
28.0 J
0.22 U
2.5 J
16.4 J
0.8 U
Accutest Laboratories • Report of Analysis Page l of l
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
MW-66
Fl2586-4
AQ -Ground Water
SW846 8260B
Project: GELS, Hendersonville, NC
Run #1
Run #2
File ID
C0008834.D
DF
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 l ,2-Dichloroethane
156-59-2 cis-l ,2-Dichloroethylene
156-60-5 trans-l ,2-Dichloroethylene
127-\8-4 Tetrachloroethylene
79-0 !-6 Trichloroethylene
75-0 l-4 Vinyl chloride
CAS No. Surrogate Recoveries
!868-53-7 Dibromofluoromethane
l 7060-07-0 l ,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromot1uorobenzene
ND = Not detected
RL = Reporting Limit
Analyzed By
03/15/02 JG
Result
ND
0.85
ND
ND
ND
61. !
ND
ND
Run# 1
105%
106%
-98%
100%
E = lndicJtes value exceeds calibr:ition range
RL
l.O
2.0
2.0
2.0
2.0
2.0
2.0
1.0
Run#2
Date Sampled: 03/12/02
Date Received: 03/13/02
Percent Solids: nfa
Prep Date
n/a
Units Q
ugil
ugil J
ug/1
ug/t
ug/1
uo:'1 o·.
ug_rl
ugil
Limits
80-120%
30-120%
80-120%
80-120%
Prep Batch
n/a
Analytical Batch I
VC-104
J = Indicates an t!stimated value ! r;_ ... ';';
B = Indicates analyte found in associated ,,\J..hell blank
N = Indicates presumptive evidence of a compound
011
Accutest Llboratories
Client Sample ID:
Lab Sample ID:
MatrLx:
MW-66
F\2586-4
•
AQ -Ground Water
Report of Analysis
Date Sampled: 03/12/02
Date Received: 03/ 13/02
Percent Solids: n/a
PJge l of l
Project: GELS. Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units DF Prep Analyzed By Method Prep '.lethod
Barium 28.0"B.. °1 l.200 0.94 ug/1 03/14/02 03/15/02 DM SW846 60108 SW846 3010A
Beryllium 0.22 U 5.0 0.22 ug/1 03/14/02 03/ I 5/02 DM SW846 60!08 SW846 3010.-\
Lead 2.s 1:1---J l..5 o l.2 ug/1 03/ 14/02 03/ I 5/02 DM SW846 60108 SW846 3010.<
Manganese 16.4 "J') 15 0.26 ug/1 03/14/02 03/15/02 DM SW846 60!0B SW846 2010.-\
Nickel 0.80 U 40 0.80 ug/1 03/14/02 03/15/02 OM SW846 60108 SW846 3010.-\
c/(x),v
'
RL = Reporting Limit C = Indicates a result< IDL
IDL = Instrument Detection Limit B = Indicates a result > = IDL but < RL
020
Table D-2. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remedialion
Parameter Goal
voe, (µg/L)
1,2-Dichloroethane
Benzene
Chlurofonn
cis-1,2-Dich!orot::thene
Tetrachloroethene
trans-1,2-Dich!oroethene
Trichloroethene
Vinyl ch\oridt:
SVOCs (ftg/L)
Nitrobcnzc:nc
METALS TOTAL (flg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND • not detected
J • detected, estimated result
UJ • not detected, estimated result
0 • dilution sample
E · exceed calibration limit
B •found in blank
70
70
2.8
10
2000
4
15
50
100
RWSF-1
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND ( 1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0)
ND(2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0J
ND (2.0) ND (2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0)
34.0 51.-1 43.2 0 40.4 46.3 52.6
ND (2.0) ND (2.0) ND (2.0) ND (2 OJ ND (2.0) ND (2.0)
ND (2.0) ND('.LO) ND (2.0) ND (2.0) ND (2.0J ND(2.0)
ND(l.0) ND ( 1.0) ND (1.0) ND(l.0) ND ( I.~) ND ( I.OJ
ND (5.0) ND (5.0) ND (5.5) ND(5.5) ND (5.0J ND (5.0J
161.0 J 193.0 J 290 242.0 254.0 J 153.0 J
0.3 U 2.6 UJ 2.2 U 2.3 U I. I J 1.2 J
1.5 J 50.6 J 49.5 21.4 24.3 10.4U
65.6 42.6 J 109.0 J IOO.O 90.1 J 71.8 J
13.7 J 1.4 J 6.5 J 0.8 U 3.5 J 1.8 J
Boldcd valw::s indicate dc:tectcd concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
ND (2.0)
ND (1.0)
0.52 J
ND (2.0) • 56.3
ND (2.0)
ND (2.0)
ND (I.OJ
156.0 J
0.22 U
26.1
98.1 J
4.2 J
Accutest Laboratories •
Report of Analysis Page l oi l
Client Sample ID: RWSF-l
Lab Sample ID: Fl2586-3
Matrix:
Method:
AQ -Ground Water
SW846 8260B
Project: GELS, Hendersonville, NC
Run #l
Run #2
File ID
C0008833.D
OF
VOA TCL List
C.-1.S No. Compound
71-43-2 Benzene
67-66-3 CJ.loroforrn
107-06-2 l ,2-Dichloroethane
156-59-2 cis-l ,2-Dichloroethylene
156-60-5 trans-l ,2-Dichloroethylene
[27-18-4 TerracWoroethylene
79-0 l-6 TncWoroethylene
75-0l-4 Vinyl chloride
C.-1.S No. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
l 7060-07-0 l ,2-DicWoroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromofluorobenzene
ND = Not detected
RL = Reporting Limit
Analyzed By
03/15/02 JG
Result RL
ND \.0
0.52 2.0
ND 2.0
ND 2.0
ND 2.0
56.3 2.0
ND · 2.0
ND l.O
Run# 1 Run#2
i65%
106% •
99%
%%
E = Indicates value exceeds calibration range
Date Sampled: 03/\2/02
Date Received: 03/13/02
Percent Solids: n/a
Prep Date
n/a
'Cnits Q
ug/1
ug!l J
ug!l
ugfl
ug!l
ug/1
ug!l
ug/l
Limits
80-120%
80-120%
30-120%
80-120%
Prep Batch
n/a
Analytical Batch
VC404
J = Indicates an estimated value
B = Indicates onalyte found in associated method blank
N = lndicates presumptive evidence of a~ pllup<i Q l (} J,_.1. •
Accutest Laboratories •
Client Sample ID: RWSF-1
Lab Sample ID: F\2586-3
Matrix: AQ -Ground Water
Report of Analysis
Date Sampled: 03/ l 2/02
Date Received:. 03/13/02
Percent Solids: nh
Page l of I
Project: GELS. Hendersonville. NC
Metals Analysis
Analyte Result RL IDL Units
Barium 156 'B-,, -S}; 200 0.94 ug/1
Beryllium 0.22 U 5.0 0.22 ug/1
Lead 26. l 5.0 1.2 ug/1
~iang::mese 98.l J\ 15 0.26 ug/1
Nickel 4.2"B....j} 40 0.80 ug/1
RL ; Reporting Limit
!DL ; Instrument Detection Limit
DF Prep Analyzed By Method Prep '.\,lethod
03/14/02 03/15/02 DM SW846 6010B SW846 3010A
03/14/02 03/15/02 OM SW846 6010B SWS-16 3010.-\
03/14/02 03/15/02 DM SW846 6010B SWS46 ,0!0A
03/14/02 03/15/02 DM SW846 6010B SWS46 3010.,
03/14/02 03/15/02 OM SW846 60\0B SW846 !0!0A
U ; Indicates a result < !DL 1,, 1 -,
B ; Indicates a result >; !DL but-'< RL
019
North Carolina •
Department of Environment and Natural
Resources
Michael F. Easley, Governor
William G. Ross Jr., Secretary
Dexter R. Matthews, Director
Ms. Giezelle Bennett
Superfund Branch
Waste Management Division
April 16, 2002
United States Environmental Protection Agency
Region IV
61 Forsyth Street, 11 th Floor
Atlanta, Georgia 30303
RE: Groundwater Sampling Results -Dr. Gary Hill
General Electric/Shepherd Farm NPL Site
East Flat Rock, Henderson County
Dear Ms. Bennett:
The Superfund Section of the North Carolina Department of Environment and Natural Resources
(NC DENR) received the Groundwater Sampling Results for Dr. Gary Hill for the General
Electric/Shepherd Farm National Priorities List (NPL) Site. The Superfund Section has reviewed
this document and offers the following comments.
Groundwater Sampling Results -Dr. Gary Hill
1. Table 1 -Shepherd Farm Subsite-Performance Well Analytical Results indicates that the
September 2000 groundwater sample collected from monitoring well MW-64A contained
no detectable concentrations oflead at a laboratory detection limit of 12.0 micrograms per
liter ( g/L). However, the attached laboratory documentation indicates that the September
2000 groundwater sample collected from monitoring well MW-64A contained no detectable
concentrations of lead at a laboratory detection limit of 1.2 g/L. Please clarify this
discrepancy.
2. Table I -Shepherd Farm Subsite -Performance Well Analytical Results indicates that the
September 2000 groundwater sample collected from monitoring well MW-64A contained
90. 7 g/L manganese. However, the anached laboratory documentation does not include
the results of any analyses for manganese on the September 2000 groundwater sample
collected from monitoring well MW-64A. Please clarify this discrepancy.
1646 Mail Service Center, Raleigh, North Carolina 27699-1646
Phone: [phone] \ FAX: [phone] \ Internet: ,v,,vw.em.state.nc.us
AN EQUAL OPPORTUNITY\ AFFIRMATIVE ACTION EMPLOYER-50% RECYCLED/ 10% POST CONSUMER PAPER
Ms. Giezelle Bennett
April 16, 2002
Page 2
•
We appreciate the opportunity to comment on this document. If you have any questions, please feel
free to call me at [phone], extension 349.
Sincerely,
[) a1.fLci 8 . fl'i oX}._;__n ,?'~/ J_jc_
David B. Mattison, CHMM
Environmental Engineer
Superfund Section
Sent ,\y: HSI GeoTre.ns; 7706428808; Apr-24-02 10:00AM; Pe.ge 4/5 •
Accu1csl LabLink@I 3262 09:42 19-Apr-2002
Report of Analysis Pr.ge I of I
Client Sample ID: MW-64A
Lab Sample ID: F77_14-_1
Malrh: AQ -Grountl Water
Project: GELS, Hcmlcnuuvilk:, NC
Metal• Analysis
Analytc Result RL Units DF
Bnriun1 34.0 B 200 ug/1
Oeryllillm 0. 79 B 5.0 ug/1
Lextl 12 U o 0 ug/1
Mnngn.nese 90.7 I'-I) ug/1
Nickel !9B 4() 0 ug/1
RL ~ lleporting LimiL
!'rep
09/29100
09/29/00
09/29/00
09129/00
09/29/00
Date Sampled: 09127/00
Dale Received: 09/28100
Percent Solids: nla
Analy,ed By Method
10102100 JK SW&46 GO I (J~
10/02100 JK SW846 ()lll(JU
I 0/02/00 JK SWH46 t>UJOB
10/02/00 JK SW846 60HlB
I 0102/00 JK SW34Ci (,ll)OU
Prep Metliud
SWS46 3010A
SW8Mi 101UA
SW!i4<i 3010/\
SW846 3010A
SW84~ 301t1A
12 uf 46
Table D-1. GE StJbsite -Pe<fonnance Weli Analytical Results. (continued)
Remediation
MW-64A
Parameter Goal Sep-00 Dec-00 Mar--01 Jun-01 Sep--01 Mar-02 Juo-02 Sep-02 Dec-02
--------.. -----------------
l ,2-Dichlon:rth.a:,e N l1 (2.0) ND (2.0) ND (2.0) ND (20) oD(2.0) ND(l.0)
---· -----·------
ND(!D) ND (Lo:, N!l (l.0) ND (1.0) NDO.O) ~D {' .. D)
---· ·---·---· -------------------
ChlcrrofO'Tffl ND (2.0) ND(l-0'! ND (2.0) O.<>!!J 0.'561 NU (2.0)
-------· ------· ----------
ci1-1.2-Dii:hloroc:Ulene 70 1'D (2.0) ND (2.0J l<D (). ()) ND (2.0) ND (l O) ND(2.0)
---· ------------·-
1 etue,hloroe:t.hcrx: 50.2 46.7 43.) 4U! 42.8 41.8
---------· --· ·--· ·---
lra!ly-1,2-Di-cbloroctheoe 70 1'D (2.0) ND (2.0) 1'D (2.•)) ND (2.0) ND (2 D) ~D(.2.0'!
------··------· ---·-
1 tichlorncthene ~.8 ND (2.0) 1'D (2 O) ND (2.0) ND (1.0) KD(20) NU (2 0)
--------· -------------
Vinyl crtlor-ide 1'D (I.OJ ND ,:1.0) XD (l.0) ND(l.0) ND (l.O) ;\O (l .OJ
------·· ---··--· ----
svoc. (µg/L) ----------------·------. ---·-----------------·--· ·-----· ·--.
Nitrot>Cll7.rnC JO ND (c.O) ND (S.0) ND (5.0) ND(1.0j
----·---·---· ---·-------
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Nickel
.....,,
U,ND • no\ dittected
J • dl!ltcted, li'5timatt!d nisutt
U J • ACX de1iected. e, t:m .rt:ed. ~, u It
V, dllU'IJon samp~
E -nceed aiiib-raticri llmrt
6 • found iri bb.:nk
2000 H.0'
4 0.79U
15 uu
50 91.7 -----
100 I .CJ l1
-------· ------.•--·---
J 3.6 J 36.0 J 32. 7 J 29.7 J 30 l J
·------------·---
0.86 UJ 0.76U 0.83 U 0.6U 0.22 U --------------------
1.1 UJ 1 . .': U l.4U 1.2 J HU
---· -----------· ---------
76.9J 9!..4J 70.8 -51,4 J 50.4
-------· ---· ---· ------
0. B L1J 0.97 J 0.8U 0.8 U 0.& U
·-------------· ---------
--c------------------
BolC-ed value:-indicate detected c:oote.JJtrations great.cs-th.a.n ~iarion gc-ah,
rl
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Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichlorocthane
Benzene
Chlorofonn
cis-1,2-0ichloroethene
Tetrachloroethcne
trans-1,2-Dichlorocthene
Trich\oroethene
Vinyl chloride
SVOCs (µg/L)
Nitrobenzcne
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND • not detected
J -detected, estimated result
UJ -not detected, estimated result
D -dilution sample
E • exceed calibration limit
B -found in blank
70
70
2.8
10
2000
4
15
50
100
MW-66
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0) NLJ (I.OJ
ND (2.0) ND (2.0) 0.81 J ND (2.0) 0.77 J ND (2.0)
1.6 J ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
23.2 J 45.8 53.4 54.5 65.7 58.5
NLJ (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
0.94 J ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND(I.0)
ND (5.0) ND (5.0) ND (5.5) ND (5.0) ND (5.0) ND (5.0)
52.3 J 36.1 J 39.6) 26.0 J 40.0 J 39.2 J
1.5 U 0.87 UJ 0.8 U 0.94 U 0.81 U 0.22 U
4.2 J 1.6 UJ 3.SU 1.6 U 1.9 J 6.] U
223 57.J J 81.2 20.4 119.0 J 98.9
5.3 U I.SJ 1.8 U 0.8 U 1.2 J 1.9 J
Balded values indicate detected concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
•
l~ccuTEST. •
Client Sample ID: :V!W-66
Lab Sample ID: F7734-5
Matrix: AQ -Ground Water
Method: SW846 8260B
Report of Analysis
Date Sampled: 09/27 /00
Date Received: 09/28/00
Percent Solids: n/a
Project: GELS, Hendersonville, NC
Run . .:¥ l
Run.#2
File ID
C0000741.D
OF
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 1.2-Dichioroethane
156-:59-2 cis-1.2-Dichloroethytene
156-60-5 trans-1.2-Dichloroethylene
127-18-4 T etrachloroethylene
79-01-6 Tric~loroethylene
75-01.:+ Vin:11 chloride
CAS No. Surrogate Recoveries
1868-53-7 Di b romo t1uoro methane
17060-07-0 l. -~ -Dichloroethane-D4
2037-26-5 Toluene-DS
460-00-4 4-Bromorluorobenzene
. .\nalyzed By
10106100 JG
Result RL
ND 1.0
ND 2.0
ND 2.0
1.6 :.o
ND 2.0
13.2 2.0
0.94 2.0
ND 1.0
Prep Date
n/a
Units Q
ug/1
ugfl
ug/1
ug/l J
ug/1
ug/1 --J
ug/1 J
ug/1
Prep Batch
n/a
Run# 1 Run# 2 Limits
100% 30-120%
93% 69-128%
97% 80-120%
92% 80-120%
J = Indicates an estimated value
Page I oi I
Analytical Batch
YC30
ND = Not detected
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound r, 1 7
·• f"i-'\~ '-.,_ I
Florida • .l405 1/inelallC Road· Suite.C-i5 ·Orlando.Fl 32811 • :el: JQl-425:6700 • lax: AQ7.J25-!}7,j7 • hrtp"//www.accutest.com
i2ccUTEST. •
Report of Analysis Page l of l
Client Sample ID: MW-66
Lab Sample ID: F7734-5
Matrix:
Method:
Project:
AQ -Ground Water
SW846 35 l0C/8270C
GELS, Hendersonville, NC
File ID
WC02700.D
DF Analyzed By
Run #1
Run #2
ABN TCL List
CAS No.
98-95-3
C..\..5 :\o.
367-12-4 .
4 [65-62-2
118-79-6
4[65-60-0
321-60-8
17[8-51-0
Compound
Nitrobenzene
Si..:.rro~:ite Recoveries
2-Fluorophenol
Phenoi-d5
2,-l ,6-Tribromophenol
Nicrobenzene-d5
2-Fiuorobiphenyl
Terphenyl-cil4
ND = Not detected
RL = Reporting Limit
l0/09/00 ME
Result RL
ND 5.0
RunJ l Run,/::
57%
35%
91 %
96%
91 %
96%
E = Indicates value exceeds calibration range
Date Sampled: 09127100
Date Received: 09/28/00
Percent Solids: n/a
Prep Date
10/03/00
Units Q
ug/1
Limits
2!-l00%
l0-94%
10-123%
35-114%
43-116%
33-14[%
Prep Batch
OP2129
I = Indicates an estimated value
Analytical Batch
SW!64
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound r. ') r
.,_; .,J ..
Florida• 4405 Vineland ?.oad •·Suite C-15 ·Orlando.FL 32811 • te!: 407-425-6700 • fax: 407-J25-07G7 • htto:/fwwwaccutest.com -· .... --018
~r!i •
;aACCUTEST.
Client Sample ID:
Lab Sample ID:
Matrix:
MW-66
F7734-5
AQ -Ground Water
Report of Analysis
Date Sampled:
Date Received:
Percent Solids:
09/27/00
09/28/00
n/a
Project: GELS, Hendersonville, NC
:Vletals Analysis
Analyte Result RL Units DF Prep Analyzed By Method
Barium 52.3 B-.. )2:. 200 ug/1 09/29/00 10/02/00 JK SWS46 60l08
Beryllium l.5R_ V \ 5.0 ug/l 09/29/00 l0/02/00 JK SW846 6010B
Lead 4.2 B--J.;, 5.0 ug/1 09/29/00 10/02/00 JK SW846 60l0B
Manganese 223 15.0 ug/l 09/29/00 l0/02/00 JK SWS46 60l0B
Nickel 5.3 lL\J\ 40.0 ug/1 09/29/00 l0/02/00 JK SW346 60l0B
RL = Reporting Limit
..
· Florida • 4J05 Vineland ?.oao • Suite C-15 • Orlanc:o. Fl 32311··• tel: 407, 425-6700 • .fa.x: ..:07-425-07Ci • hno://www accutest.com
Page I of l
046
•
Report of Analysis Page l of l
Client Sample ID: MW-66
Lab Sample ID: F8302-2
t\'latrix: AQ • Ground Water
Method: SW846 82608
Project: GELS, Hendersonville, NC
File ID DF
Run #l C000l6l3.D l
Run #2
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 l .2-Dichloroethane
156-59-2. cis-1,2-Dichloroethylene
156-60-5 trans-l ,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-0 l-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Dibromotluoromethane
l 7060-07-0 1,2-Dichloroethane-D4
2037-26-5 Toluene-OS
460-00-4 4-Bromotluorobcnzene
ND = Not detected
RL = Reporting Limit
Analyzed
12/07/00
Result
ND
ND
ND
ND
ND
45.8
ND
ND
Run# I
96%
100%
103%
101 %
E = Indicates value exceeds calibration range
Date Sampled: l 2/05/00
Date Received: l 2/06/00
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
JG n/a n/a VC73
RL Units Q
1.0 ug/1
2.0 ug/1
2.0 ug/1
2.0 ug/1
2.0 ugil
2.0 ug/l
2.0 ug!l
1.0 ug/1
Run# 2 Limits
80-120%
69-128%
80-120%
80-120%
J = lndicates an estimated value
B = Indicates analyte found in associated method blank
N = [ndicates presumptive evidence of a compound
,,JS
. '-'
Report of Analysis Page I of 1
Client Sample ID: MW-66
Lab Sample ID: F8302-2
i\.-latrix:
Method:
Project:
AQ -Ground Water
SW846 8270C SW846 35 I 0C
GELS, Hendersonville, NC
File ID
W003267.D
OF Analyzed By
Run #l
Run #2
ABN TCL List
CAS No. Compound
98-95-3 Nitrobenzene
CAS No. Surrogate Recoveries
367-12-4' 2-Fluorophenol
4165-62-2 Phenol-d5
l 18-79-6 2,4,6-Tribromophenol
4 I 65-60-0 Nitrobenzene-d5
321-60-8 2-Fluorobiphenyl
1718-51-0 Terphenyl-d 14
ND = Not detected
RL = Reporting Limit
12/08/00 ME
Result RL
ND 5.0
Run# I Run# 2
46%
27%
79%
84%
84%
91%
E ;:::: Indicates value exceeds calibration range
Date Sampled:
Date Received:
Percent Solids:
12/05/00
12/06/00
n/a
Prep Date
12/07/00
Prep Batch
OP2404
Units Q
ug/1
Limits
21-100%
10-94%
10-123 %
35-114%
43-116%
33-141%
J = Indicates an estimated value
Analytical Batch
SWl95
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compQU,Qd 1~}:l.
Ci\'rn!IQ • biJILI
[jACCUTEST.
Client Sample ID: M W-66
Lab Sample ID: F8302-2
t\latrb:: AQ -Ground Water
Report of Analysis
Date Sampled:
Date Received:
12/05/00
12/06/00
Percent Solids: n/a
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL Units OF Prep Analyzed By Method
Barium 36 1,1,".J 200 ug/1 12/07/00 12/14/00 JK SW8~6 60108
Beryllium 0.87 ,5' u:r 5.0 ug/1 12/07100 12/14/00 JK SW846 60108
Lead t.6J.-VT 5.0 ug/1 12/07 /00 12/14/00 JK SW846 60108
Manganese 57.3 ':f" 15.0 ug/1 12107 /00 12/14/00 JK SW846 6010B
Nickel 1.8)ii .J 40.0 ug/1 12/07100 12/14/00 JK SWS46 60108
~ s,a._""i'U-net f•Ltce·,\'\ f,-e,c,e,,-J-u:)..j •.
('f'\ n ·\-0 C-s..,__,; :~\ CL\ \-_,Tic" '7 IC ,-6 o\.:.* .
IY\ S \ (h ',; \/ , c,_ C .
Q?v
\J-
RL = Reporting Limit
Page I of I
ti.0
•
Report of Analysis Page l of l
Client Sample ID: MW-66
Lab Sample ID: F9!96-3
Matrix: AQ -Ground Water
Method: SW846 8260B
Project: GELS, Hendersonville, NC
File ID DF
Run #l C0003074.D
Run #2
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107,06-2 l ,2-Dichloroethane
156-59-Z-cis-l ,2-Dichloroethylene
l 56-60-5 trans-l ,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-0 l-6 Trichloroethylene
75-0 l-4 Vinyl chloride
CAS No. Surrogate Recoveries
!868-53-7 Dibromofluoromethane
l 7060-07-0 l ,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromofluorobenzene
ND = Not detected
RL = Reporting Limit
Analyzed
03/l6/0l
Result
ND
0.81
ND
ND
ND
53.4
ND
ND
Run# 1
94%
99%
106%
100%
E = Indicates value exceeds calibration range
Date Sampled: 03/l4/0l
Date Received: 03/15/01
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
JG n/a n/a VC!45
RL Units Q
l.O ug/l
2.0 ug/l J
2.0 ug/l
2.0 ug/l
2.0 ug/l
2.0 ug/l
2.0 ug/1
l.O ug/l
Run#2 Limits
80-120%
69-128%
80-120%
80-120%
..---. ·· .. ,r,·-.. , · .... ·~(_
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
30
•
Report of Analysis Page l of l
Client Sample ID: MW-66
Lab Sample ID: F9196-3
Matrix: AQ -Ground Water
Method: SW846 8270C SW846 35l0C
Project: GELS, Hendersonville, NC
File ID DF
Run #I L006823.D l
Run #2
ABN TCL List
CAS No. Compound
98-95-3 Nitrobenzene
CAS No. Surrogate Recoveries
367-12-4 2-Fluorophenol
4165-62-2 Phenol-d5
l lS-79-6 2,4.6-Tribromophenol
4 [65-60-0 Nitrobenzene-d5
32 l-60-8 2-Fluorobiphenyl
l718-5l-0 Terphenyl-dl4
ND = Not detected
RL = Reporting Limit
Analyzed
03/20/0 I
Result
ND
Run# I
42%
28%
84%
70%
66%
l00%
E = Indicates value exceeds calibration range
By
ME
RL
5.5
Run# 2
Date Sampled: 03/l4/0l
Date Received: 03/15/0l
Percent Solids: n/a
Prep Date Prep Batch Analytical Batch
03/19/01 OP2873 SL404
Units Q
ug/l
Limits
21-100%
10-94%
l0-123 %
35-114%
43-l 16%
33-141 %
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
Client Sample ID:
Lab Sample ID:
Matrix:
MW-66
F9 I 96-3
AQ -Ground Water
Report of Analysis Page l of l
Date Sampled:
Date Received:
Percent Solids:
03/14/0 I
03/15/0 l
n/a
Project: GELS. Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units DF Prep Analyzed By Method
Barium 39:6--H' ,T 200 0.94 ug/l 03/20/0 l 03/27 /0 l JK SW846 60108
Beryllium 0. 80 .8"" '--' 5.0 0.22 ug/l 03/20/0 I 03/27/0l JK SW846 60108
Lead 3.8.!r' '--5.0 l.2 ug/1 03/20/01 03/27/01 JK SW846 60108
Manganese 8l.2 .T l5 0.26 ug/l 03/20/0 l 03/27/0l JK SW846 60108
Nickel t.8 W---s-40 0.80 ug/l 03/20/0l 03/27 /0 l JK SW846 60108
RL = Reporting Limit U = Indicates a result < IDL
ID L = Instrument Detection Limit B = Indicates a result > = IDL but < RL
Accutest Laboratories •
Report of Analysis Page 1 of 1
Client Sample ID: MW-66
Lab Sample ID: F9887-4
Matrix:
Method:
AQ -Ground Water
SW846 8260B
Project: GELS, Hendersonville, NC
Run #1
Run #2
File m
H0\2175.D
DF
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 1,2-Dichloroethane
156-59-2 cis-1,2-Dichloroethylene
156-60-5 trans-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Dibromolluoromethane
17060-07-0 1,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromolluorobenzene
ND = Not detected
RL = Reporting Limit
Analyzed
06113/01
Result
ND
ND
ND
ND
ND
54.5
ND
ND
Run# 1
107%
120%
94%
99%
E = Indicates value exceeds calibration range
By
NAF
RL
1.0
2.0
2.0
2.0
2.0
2.0
2.0
1.0
Run# 2
.. I ,-.·-i..c,•.-::-'--=--=
Date Sampled: 06105101
Date Received: 06106/0 I
Percent Solids: n/a
Prep Date
n/a
Units Q
ug/1
ug/1
ug/1
ug/l
ug/1
ug/1
ug/1
ug/1
Limits
80-120%
80-120%
80-120%
80-120%
Prep Batch
n/a
·•-:r:"", ', ;:_
'a\ 'i ,,, \ ·_cc
J = Indicates an estimated value
Analytical Batch
VH340
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compo~nd
,: } { '.-... ~ -~ ----
Accutest Laboratories •
Report of Analysis Page l of l
Client Sample ID: MW-66
Lab Sample ID: F9887-4
Matrix: AQ -Ground Water
Method: SW846 8270C SW846 35\0C
Project: GELS, Hendersonville. NC
File ID OF
Run #I W00537l.D I
Run #2
ABN TCL List
CAS No. Compound
98-95-3 Nitrobenzene
CAS No. Surrogate Recoveries
367-12-4 2-Fluorophenol
4165-62-2 Phenol-d5
l 18-79-6 2,4,6-Tribromophenol
4165-60-0 Nitrobenzene-d5
321-60-8 2-Fluorobiphenyl
1718-51-0 Terphenyl-d\4
ND = Not detected
RL = Reporting Limit
Analyzed
0611110 I
Result
ND
Run# I
52%
34%
101 %
89%
81 %
97%
E = Indicates value exceeds calibration range
Date Sampled: 0610510 l
Date Received: 06/0610 I
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch.
ME 06107101 OP3268 SW296
RL Units Q
5.0 ug/1
Run#2 Limits
20-125%
10-125%
35-140%
46-125%
46-125%
49-126%
,,-cs::
-\~/'r1· ', (2-
\ -' 7. ;,,-I()\ ' .
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of~. compound
•. .1 (1 ,q -....:,~
Accutest Laboratories
Client Sample ID: MW-66
Lab Sample ID: F9887-4
•
~latrix: AQ -Ground Water
Report of Analysis
Date Sampled: 06J05JO I
Date Received: 06J06JO I
Percent Solids: nJa
Page l of l
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units OF Prep Analyzed By Method
Barium 26.0 ff.:-200 0.94 ug/l 06/07 JO 1 06J08/01 JK SW846 60108
Beryllium 0.94.B·c.: 5.0 0.22 ug/1 06J07/0I 06J08J01 JK SW846 60108
Lead 1.6 B" ~· 5.0 1.2 ug/1 06J07 JO 1 06J08J01 JK SW846 60108
Manganese 20.4 15 0.26 ug/1 06J07 JO 1 06J08JOI JK SW846 60108
Nickel 0.80 U 40 0.80 ug/1 06J07 JO 1 06J08JO 1 JK SW846 60108
RL = Reporting Limit U = Indicates a result < ID L
ID L = Instrument Detection Limit B = Indicates a result > =· IDL but < RL :[ i 1 r::-......... ')
• Accutest Laboratories
Report of Analysis Page l of 1
Client Sample ID: MW-66
Lab Sample ID: Fl0823-3
Matrix:
Method:
AQ -Ground Water
SW846 8260B
Projeet: GELS, Hendersonville, NC
Run #1
Run #2
File ID
C0005617.D
DF
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107s06-2 1, 2-Dichloroethane
156-59-2 cis-l ,2-Dichloroethylene
156-60-5 trans-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
Analyzed By
09/12/0 I JG
Result RL
ND 1.0
0.77 2.0
ND 2.0
ND 2.0
ND 2.0
65.7 2.0
ND 2.0
ND 1.0
Date Sampled: 09/04/0 I
Date Reeeived: 09/06/01
Percent Solids: n/a
Prep Date
n/a
Units Q
ug/1
ug/1 J
ug/1
ug/1
ug/1
ug/1
ug/1
ug/l
Prep Batch
n/a
Analytical Batch
VC271
CAS No. Surrogate Reeoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromot1uoromethane 102%
17060-07-0 l ,2-Dichloroethane-D4 113%
2037-26-5 Toluene-OS 99%
460-00-4 4-Bromot1uorobenzene 97%
---'::..,
., .·r;:rr,.,c{• \'.I '~
ND = Not detected
RL = Reporting Limit
,c\?\:::ci
E = Indicates value exceeds calibration range
80-120%
80-120%
80-120%
80-120%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
Accutest Laboratories • Report of Analysis Page I of I
Client Sample ID: MW-66
Lab Sample ID: F\0823-3
r\ilatrix:
Method:
Project:
AQ -Ground Water
SW846 8270C SW846 35 I0C
GELS, Hendersonville, NC
File ID
L008964.D
DF
I
Analyzed By
Run #I
Run #2
ABN TCL List
CAS No.
98-95-3
CAS No.
367-12:4
4165-62-2
118-79-6
4165-60-0
321-60-8
1718-51-0
Compound
Nitrobenzene
Surrogate Recoveries
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
Nitrobenzene-d5
2-Fluorobiphenyl
Terphenyl-dl4
ND = Not detected
RL = Reporting Limit
09/13/01 ~IE
Result RL
ND 5.0
Run# 1 Run# 2
46%
32%
87%
71 %
70%
100%
E = Indicates value exceeds calibration range
Date Sampled: 09/04/0 I
Date Received: 09/06/0 I
Percent Solids: n/a
Prep Date
09/09/01
Units Q
ug/1
Limits
20-125%
10-125%
35-140%
46-125%
46-125 %
49-126%
Prep Batch
OP3816
J = Indicates an estimated value
Analytical Batch
SL513
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
330
• Accutest Laboratories
Report of Analysis Page l of l
Client Sample ID: MW-66
Lab Sample ID: Fl0823-3
Matrix: AQ • Ground Water
Project:
Metals Analysis
Analyte
Barium
Beryllium
Lead
Manganese
Nickel
GELS, Hendersonville, NC
Result RL IDL Units
40.0►3' 200 0.94 ug/1
0 . 8 I B""' 0 5.0 0.22 ug/1
I. 9 ff"'. .J 5.0 1.2 ug/1
l 19 3 15 0.26 ug/1
l.2 S,-_r 40 0.80 ug/l
--;;rr,,, 1... e.
OF
I ..::, \ :; ) -::_; '
RL = Reponing Limit
IDL = Instrument Detection Limit
Date Sampled: 09/04/0 l
Date Received: 09/06/0 l
Percent Solids: n/a
Prep Analyzed By Method
09/13/01 09/19/01 JK SW846 60!08
09/13/01 09/l9/0I JK SW846 60108
09/13/0 I 09/l 9/0 I JK SW846 60!08
09/13/0l 09/19/0 l JK SW846 60108
09/l3/0l 09/19/01 JK SW846 60108
U = Indicates a result < IDL
B = Indicates a result > = IDL but < RL
018
Accutest Laboratories •
Report of Analysis Page l of I
Client Sample ID: MW-66
Lab Sample ID: Fl 1780-9
Matrix: AQ: ·Ground Water
Method: SW846 8260B
Project: GELS. Hendersonville, NC
File ID DF
Run #I 80007643.D I
Run #2
VOA TCL List
CAS No. Compound
i 1-43-2 Bc:nzem:
67-66-3 Chloroform
l 07-06-2 l ,2-Dichloroethane
156-59-2. cis-1.2-Dichloroethylene
156-60-5 trans-1,2-Dichloroethylene
i27-13-~ T c:tr:i.chlorocthyk~e
79-01-6 Trichloroethylene
75-01-"1' \·inyi ~hiuriJc
CAS No. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
17060-07-0 I ,2-Dichloroethane-D4
2037-26-5 Toluene-OS
460-00-4 4-Bromofluorobenzene
ND = Not detected
RL = Reporting Limit
Analyzed
12/20/0 I
Result
ND
ND
ND
ND
ND
58.5
ND
~u
Run# I
100%
98%
100%
103%
E = [ndicates value t:xceeds calibration range
Date Sampled: 12/12/0 l
Date Received: 12/14/0l
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
JG n/a n/a VB329
RL l' nits Q
1.0 ug, l
2.0 ug/1
2.0 ug.rl
2.0 ug:'l
2.0 ugil
' a Uf. l --U
2.0 ug/1
i.O ug. i
Run# 2 Limits
80-120%
80-120%
80-120%
80-120%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
020
Accutest Laboratories • Report of Analysis Page I of I
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
Project:
MW-66
Fl 1780-9
AQ -Ground Water
SW846 8270C SW846 35I0C
GELS, Hemiersonville, NC
File ID
L0I0084.D
DF Analyzed By
Run #1
Run #2
ABN TCL List
CAS No.
98-95-3
CAS No.
367-12-4
4165-62-2
I 18-79-6
"t J.65-60-0
321-60-8
1718-51-0
Compound
i'iilrobenzenc
Surrogate Recoveries
2-Fluorophenol
Pher.ol-d5
2.4,6-Tribromophenol
:--.;irn.:ibcnzcnc:-J5
2-Fluorobiphenyl
Terphenyl-dl4
ND = Not detected
RL = Reporting Limit
12/18/01 ME
Result RL
ND 5.0
Run# l Run# 2
66%
47%
105%
101 %
98%
104%
E = Indicates value exceeds calibration range
Date Sampled:
Date Received:
Percent Solids:
12/12/01
12/14/01
n/a
Prep Date
12/17/01
Prep Batch
OP4382
Units Q
ugd
Limits
20-125%
10-125~
35-140%
~6-125::
46-125%
49-126%
J = Indicates an estimated value
Analytical Batch
SL571
I
--1'.Y
\;\;Y\ ~ \ 1/)v
00 'L
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound 032
:\ccutest Laboratories • Report of Analysis Page 1 of 1
Client Sample ID: MW-66
Lab Sample ID: F 11780-9
Matrix: AQ -Ground Water
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units
Barium 39.2 'B... Tl 200 0.94 ug/l
Beryllium 0.22 U 5.0 0.22 ug/1
Lead 6.3 !) \ 5.0 1.2 ug/1
Manganese 98.9 15 0.26 ug/1
~i1.:'...:.d 1.9 &.. 11~0 a.so ug,'i
RL ; Reporting Limit
IDL ; Instrument Detection Limit
DF
1
I
Date Sampled: 12/12/01
12/14/01
n/a
Date Received:
Percent Solids:
Prep Analyzed By Method
12/18/01 12/19/01 OM SW846 6010B
12/18/01 12/19/01 DM SW8-l6 6010B
12/18/01 l 2/ 19/01 OM SW846 6010B
12/18/0 I 12/19/0 I OM SW846 6010B
i2, i3iG i i2/i9/Ui D.\J S\.,.·3.,.0 OU lUB
U ; Indicates a result < IDL
Prep :\>lethod
SW846 3010A
SWS-t6 3010.-\
SW846 3010.-1.
SW846 3010.-1.
S\"v-~-to JUiu.--\
00 r"
B ; Indicates a result >; IDL but < RL
043
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethanc
Benzene
Chloroform
cis-1,2-Dichloroethene
Tetrachloroethcne
trans-1,2-Dichloroethene
Trichloroethene
Vinyl chloride
SVOCs (µg/L)
Nitrobenzenc
METALS TOTAL (µg/L)
Barium
Beryllium
Lead
Manganese
Nickel
Notes:
U,ND -not detected
J -detected, estimated result
UJ -not detected, estimated result
D -dilution sample
E -exceed calibration limit
B -found in blank
70
70
2.8
10
2000
4
15
50
100
RWSF-1
Sep-00 Dec-00 Mar-01 Jun-01 Sep-01 Dec-01
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (I.OJ ND (1.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
34.0 51.4 43.2 0 40.4 46.3 52.6
ND (2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND(I.O)
ND (5.0) ND (5.0) ND (5.5) ND (5.5) ND (5.0) ND (5.0)
161.0 J I 93.0 J 290 242.0 254.0 J 153.0 J
0.3 U 2.6 UJ 2.2 U 2.3 U I.I J 1.2 J
1.5 J 50.6 J 49.5 21.4 24.3 10.4 U
65.6 42.6 J 109.0 J 100.0 90.1 J 71.8 J
13.7 J 1.4 J 6.5 J 0.8 U 3.5 J 1.8 J
Balded values indicate detected concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
•
Accutest LabLink@8604 17:0,-Jan-2001
Report of Analysis @ Page l of l
Client Sample ID: RWSF-l
Lab Sample ID: F7734-l~
Matrix: AQ -Ground Water
Method: SW846 8260B
Project: GELS, Hendersonville, NC
File ID DF
Run #I C0000748.D l
Run #2
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 1,2-Dichloroethane
156-59-2 cis-1, 2-Dichloroethylene
156-60-5 trans-I, 2-Dichloroethylene
127-18,4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
17060-07-0 l ,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bro mo fluorobenzene
ND = Not detected
RL = Reporting Limit
Analyzed
10/06/00
Result
ND
ND
ND
ND
ND
34.0
ND
ND
Run# l
[01%
94%
98%
92%
E = Indicates value exceeds calibration range
By
JG
RL
1.0
2.0
2.0
2.0
2.0
2.0
2.0
1.0
Run# 2
Date Sampled: 09/26/00
Date Received: 09/28/00
Percent Solids: n/a
Prep Date Prep Batch Analytical Batch
n/a n/a VC30
Units Q
ug/l
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
Limits
80-120%
69-128%
80-120%
80-120%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
Accutest Lablink@8604 17:03 25-Jan-2001
• Report of Analysis 8 Page 1 of 1
Client Sample ID: RWSF-1
Lab Sample ID: F7734-14
Matrix: AQ -Ground Water
Method: SW846 3510C/8270C SW846 3510C
Project: GELS, Hendersonville, NC
File ID OF
Run #I W002721.D I
Run #2
ABN TCL List
CAS No. Compound
98-95-3 Nitrobenzene
CAS No. Surrogate Recoveries
367-12-4 2-Fluorophenol
4165-62-2 Phenol-d5
118-79-6 2, 4, 6-Tribromophenol
4165-60-0 Nitrobenzene-d5
321-60-8 2-Fluorobiphenyl
1718-51-0 Terphenyl-dl4
ND = Not detected
RL = Reporting Limit
Analyzed
10/10/00
Result
ND
Run# 1
57%
35%
91%
96%
88%.
93%
E = Indicates value exceeds calibration range
By
ME
RL
5.0
Run# 2
Date Sampled: 09/26/00
Date Received: 09/28/00
Percent Solids: n/a
Prep Date Prep Batch Analytical Batch
10/03/00 OP2129 SW165
Units Q
ug/1
Limits
21-100%
10-94%
10-123%
35-114%
43-116%
33-141%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
~r!i
~ACCUTEST..
Client Sample ID: R WSF-l
Lab Sample ID: F7734-l4
AQ -Ground Water
Report of Analysis
Date Sampled: 09/26/00
Date Received: 09/2S/00
Percent Solids: n/a
Project: GELS. Hendersonville. NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method
Barium l6l 'B,.,.)l 200 ug/1 l0/02/00 l0/03/00 JK SW846 6010B
Beryllium 0.3013.. V\ 5.0 ug/l l0/02/00 l0/03/00 JK SWS46 6010B
Lead l.5'B.. 31., 5.0 ug/1 l0/02/00 l0/03/00 JK SWS46 6010B
Manganese 65.6 15.0 ug/1 10/02/00 l0/03/00 JK SWS46 60108
Nickel l3.7B.. 3'.}__-10.0 ug/l l0/02/00 l0/03/00 JK SW846 60108
RL = Reporting Limit
f!nrida . .--:44QS-l/ine1ana Roaa • Suite C-15 • Orlando. Fl: )28\.1 • tel: .t07-J25-6700 • 1~: 40?. J25-07~7 • hno://www.accutest.com
Page l of l
C55
•
Report of Analysis Page l of l
Client Sample ID: RWSF-1
Lab Sample ID: F8302-l
Matrix: AQ. Ground Water
Method: SW846 8260B
Project: GELS. Hendersonville, NC
File ID DF
Run #I C000I6l2.D I
Run #2
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 1,2-Dichloroethane
I 56:59-2· · cis-1,2-Dichloroethylcne
I 56-60-5 trans-1,2-Dichloroethylene
127-18-4 Tetrachloroeth ylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Dibromot1uoromethane
17060-07-0 1,2-Dichloroethane-D4
2037-26-5 Toluene-OS
460-00-4 4-Bromot1uorobenzcne
ND = Not detected
RL = Reporting Limit
Analyzed
12/07/00
Result
ND
ND
ND
ND
ND
51.4
ND
ND
Run# I
97%
!00%
104%
99%
E = Indicates value exceeds calibration range
By
JG
RL
1.0
2.0
2.0
2.0
2.0
2.0
2.0
1.0
Run# 2
Date Sampled: I 2/05/00
Date Received: 12/06/00
Percent Solids: n/a
Prep Date Prep Batch Analytical Batch
n/a n/a VC73
Units Q
ug/1
ug/l
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
Limits
80-120%
69-128%
80-120%
80-120%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
Report of Analysis Page I of 1
Client Sample ID: RWSF-1
Lab Sample ID: F8302-I
Matrix: AQ -Ground Water
Method: SW846 8270C SW846 35 I0C
Project: GELS, Hendersonville, NC
File ID DF
Run #I W003266.D l
Run #2
ABN TCL List
CAS No. Compound
98-95-3 Nitrobenzene
CAS No. Surrogate Recoveries
367-12-4 2-Fluorophenol
4165-62-2 Phenol-d5
118-79-6 2,4,6-Tribromophenol
4165-60-0 Nitrobenzene-d5
321-60-8 2-Fluorobiphenyl
1718-51-0 Terphenyl-d 14
ND = Not detected
RL = Reporting Limit
Analyzed
12/08/00
Result
ND
Run# I
56%
35%
84%
93%
93%
92%
E = Indicates value exceeds calibration range
By
ME
RL
5.0
Run# 2
Date Sampled: 12/05/00
Date Received: 12/06/00
Percent Solids: n/a
Prep Date Prep Batch Analytical Batch
12/07/00 OP2404 SWl95
Units Q
ug/1
Limits
21-100%
10-94%
10-123%
35-114%
43-116%
33-141%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound......-,
·1},'
~r!'t •
;:jACCUTEST.
Client Sample ID: R WSF-1
Lah Sample ID: F8302-I
Matrix: AQ -Ground Water
Report of Analysis
Date Sampled:
Date Received:
12/05/00
12/06/00
Percent Solids: nfa
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL lJnits DF Prep Analyzed By Method
Barium 193 . .r' S 200 ug/1 12/07 /00 l 2/ 14/00 JK SW846 60l08
Beryllium 2.6;.-v:3' 5.0 ug/1 12/07 /00 12/14/00 JK SW846 60108
Lead 50.6 I 5.0 ug/1 12/07 /00 12/14/00 JK SW846 60108
Manganese 42.6 ::r 15.0 ug/1 12/07/00 12/14/00 JK SW846 60 IDB
Nickel lAl'i..T' 40.0 ug/1 12/07 /00 12/14/00 JK SW846 60108
j
~'v'e.
I \'M \CI
R L ~ Reporting Limit
Page l of l
•
Client Sample ID: RWSF-1
Lab Sample ID: F9 l 99-1
Matrix:
Method:
AQ -Ground Water
SW846 8260B
Report of Analysis
Date Sampled: 03/14/01
Date Received: 03/15/01
Percent Solids: n/a
Page l of l
Project: GELS, Hendersonville, NC
Run #I
Run #2
File ID
C0003077.D
DF
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 1.2-Dichloroethane
156,59-2 cis-1,2-Dichloroethylene
156-60-5" trans-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Dibromotluoromethane
17060-07-0 I, 2-Dichloroethane-D4
2037-26-5 Toluene-DB
460-00-4 4-Bromofluorobenzene
ND = Not detected
RL = Reporting Limit
Analyzed By
03/16/01 JG
Result RL
ND 1.0
ND 2.0
ND 2.0
ND 2.0
ND 2.0
43.2 2.0
ND 2.0
ND 1.0
Run# I Run#2
96%
IOI%
105%
95%
,,.---...
Prep Date
n/a
Units Q
ug/1
ug/l
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
Limits
80-120%
69-128%
80-120%
80-120%
Prep Batch
n/a
\ ,_-:-,"; ,, ~-,~
J = Indicates an estimated value
Analytical Batch
VCl45
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
1.1
• Report of Analysis Page I of I
Client Sample ID: RWSF-1
Lab Sample ID: F9199-l
Matrix: AQ -Ground Water
Method: SW846 8270C SW846 3510C
Project: GELS, Hendersonville, NC
File ID DF
Run#! L006828.D I
Run #2
ABNTCL List
CAS No. Compound
98-95-3 Nitrobenzene
CAS No. Surrogate Recoveries
367:12-4. 2-Fluorophenol
4165-62-2 Phenol-d5
118-79-6 2,4,6-Tribromophenol
4165-60-0 Nitrobenzene-d5
321-60-8 2-Fluorobiphenyl
1718-51-0 Terphenyl-d\4
ND = Not detected
RL = Reporting Limit
Analyzed
03/20/0 I
Result
ND
Run# l
45%
32%
87%
74%
72%
93%
E = Indicates value exceeds calibration range
By
ME
RL
5.5
Run# 2
Date Sampled: 03/14/01
Date Received: 03/ 15/01
Percent Solids: n/a
Prep Date Prep Batch Analytical Batch
03/19/01 OP2873 SL404
Units Q
ug/1
Limits
21-100%
10-94%
10-123 %
35-114%
43-116%
33-141 %
J = Indicates an estimated value
B = Indicates anal yte found in associated method blank
N = Indicates presumptive evidence of a compound
88
Client Sample ID: R WSF-1
Lab Sample ID: F9 l 99-l
•
Matrix: AQ -Ground Water
Report of Analysis
Date Sampled: 03/14101
Date Received: 03/1510 l
Percent Solids: n/a
Page l of 1
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units OF Prep Analyzed By Method
Barium 290 200 0.94 ug/1 03120101 03/27/01 JK SW846 60108
Beryllium 2.2B'U 5.0 0.22 ug/1 03120101 03/27101 JK SW846 60108
Lead 49.5 5.0 1.2 ug/1 03/20/01 03/27 /0l JK SW846 60!08
Manganese 109 J'. 15 0.26 ug/1 03/2010 I 03/27 /0 I JK SW846 60!08
Nickel 6.5 JY). 40 0.80 ug/1 03/20/01 03/27101 JK SW846 60!08
RL = Reporting Limit U = Indicates a result < IDL
IDL = Instrument Detection Limit B = Indicates a result > = IDL but < RL
1.,G
Accutest Laboratories •
Report of Analysis Page I of I
Client Sample ID: RWSF-1
Lab Sample ID: F9887-3
I\latrix: AQ -Ground Water
Method: SW846 8260B
Project: GELS, Hendersonville, NC
File ID DF
Run #I C0004291.D I
Run #2
VOA TCL List
CAS No, Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 I, 2-Dichloroethane
156C59-2_ cis-1,2-Dichloroethylene
156-60-5 trans-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CAS No, Surrogate Recoveries
I 868-53-7 Dibromot1uoromethane
17060-07-0 l ,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromot1uorobenzene
ND ; Not detected
RL ; Reporting Limit
Analyzed
06/19/01
Result
ND
ND
ND
ND
ND
40.4
ND
ND
Run# I
88%
96%
111%
97%
E ; Indicates value exceeds calibration range
Date Sampled: 06/05/01
Date Received: 06/06/0 I
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
JG n/a n/a VC208
RL Units Q
1.0 ug/l
2.0 ug/l
2.0 ug/1
2.0 ug/1
2.0 ug/1
2.0 ug/1
2.0 ug/1
1.0 ug/1
Run# 2 Limits
80-120%
80-120%
80-120%
80-120%
' ... .:__. --=--· . '."~r; .,, ·• ,-.:...
, \ ., ., I;::. \ -. -'.
J ; Indicates an estimated value
B ; Indicates analyte found in associated method blank
N ; Indicates presumptive evidence of a cornpp'ilnd _, ~ _;
Accutest Laboratories •
Report of Analysis Page l of l
Client Sample ID: RWSF-1
Lab Sample ID: F9887-3
Matrix: AQ -Ground Water
Method: SW846 8270C SW846 3510C
Project: GELS, Hendersonville, NC
File ID DF
Run #I W005370.D I
Run #2
ABN TCL List
CAS No.
98-95-3
CAS No.
367-12-4
4165-62-2
I 18-79-6
4165-60-0
321-60-8
1718-51-0
Compound
Nitrobenzene
Surrogate Recoveries
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
Nitrobenzene-d5
2-Fluorobiphenyl
Terphenyl-dl4
ND = Not detected
RL = Reporting Limit
Analyzed
06/11/01
Result
ND
Run# l
57_%
39%
102%
98%
88%
97%
E = Indicates value exceeds calibration range
By
ME
RL
5.5
Run# 2
Date Sampled: 0610510 I
Date Received: 06/06/0 I
Percent Solids: n/a
Prep Date Prep Batch Analytical Batch
06/07 /0 I OP3268 SW296
Units Q
ug/1
Limits
20-125%
10-125%
35-140%
46-125%
46-125%
49-126%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
..-.:::• .,': r.:-......,, ...i....__)
Accutest Laboratories
Client Sample ID: RWSF-1
Lab Sample ID: F9887-3
•
Matrix: AQ -Ground Water
Report of Analysis
Date Sampled: 06/05/0 I
Date Received: 06/06/0 I
Percent Solids: n/a
Page I of I
Project: GELS, Hendersonville. NC
Metals Analysis
Analyte Result RL IDL
Barium 242 200 0.94
Beryllium 2.3B"'c.•· 5.0 0.22
Lead 21.4 . 5.0 1.2
Manganese 100 15 0.26
Nickel 0.80 U 40 0.80
c::_L_
RL = Reporting Limit
ID L = Instrument Detection Limit
Units OF
ug/1
ug/l
ug/1
ug/1
ug/1
':-
', -·
Prep Analyzed By Method
06/07 /0 I 06/08/0 I JK SW846 60108
06/07/01 06/08/01 JK SW846 60108
06/07 /0l 06/08/01 JK SW846 60108
06/07/01 06/08/01 JK SW846 60108
06/07 /0 I 06/08/01 JK SW846 60108
U = Indicates a result < ID L
B = Indicates a result > = IDL but < RL
," l _., ,,.., ,.·_.._,.;..,
• Accutest Laboratories
Report of Analysis Page l of \
Client Sample ID: RWSF-l
Lab Sample ID: FI 0823-1 Date Sampled: 09/04/0l
Matrix: AQ -Ground Water Date Received: 09/06/0 l
Method: SW846 8260B Percent Solids: n/a
Project: GELS, Hendersonville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #l C00056l5.D I 09/l 2/0 I JG n/a n/a VC27l
Run #2
VOA TCL List
CAS No. Compound Result RL Units Q
7 l-43-2 Benzene ND 1.0 ug/l
67-66-3 Chloroform ND 2.0 ug/l
107,06-2 l ,2-Dichloroethane ND 2.0 ug/1
l 56-59-2 -cis-1,2-Dichloroethylene ND 2.0 ug/1
156-60-5 trans-1,2-Dichloroethylene ND 2.0 ug/1
127-18-4 Tetrachloroethylene 46.3 2.0 ug/1
79-0 l-6 Trichloroethylene ND 2.0 ug/1
75-01-4 Vinyl chloride ND 1.0 ug/l
CAS No. Surrogate Recoveries Run# I Run# 2 Limits
I 868-53-7 Dibromolluoromethane 102% 80-120%
l 7060-07-0 l ,2-Dichloroethane-D4 ll4% 80-l20%
2037-26-5 Toluene-D8 99% 80-l20%
460-00-4 4-Bromofluorobenzene 90% 80-l20%
/--,.
~ . ·? --c'Y:·lt'-
1c \ -5\s:,:,
ND = Not detected
RL = Reponing Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
1
Accutest Laboratories • Report of Analysis Page I of I
Client Sample ID: RWSF-1
Lab Sample ID: FI 0823-1
t\,latrix:
Method:
Project:
AQ -Ground Water
SW846 8270C SW846 3510C
GELS, Hendersonville, NC
File ID
L008962.D
DF Analyzed By
Run #I
Run #2
ABN TCL List
CAS No,
98-95-3
CAS No.
367-12-4.
4165-62-2
118-79-6
4165-60-0
321-60-8
1718-51-0
Compound
Nitrobenzene
Surrogate Recoveries
2-F!uorophenol
Phenol-d5
2,4,6-Tribromophenol
Nitrobenzene-d5
2-Fluorobiphenyl
Terphenyl-dl4
ND = Not detected
RL = Reporting Limit
09/13/01 ME
Result RL
ND 5.0
Run# l Run# 2
49%
36%
94%
82%
76%
IOI%
E = Indicates value exceeds calibration range
Date Sampled: 09/04/0 I
Date Received: 09/06/0 I
Percent Solids: n/a
Prep Date
09/09/01
Units Q
ug/1
Limits
20-125%
10-125%
35-140%
46-125%
46-125%
49-126%
Prep Batch
OP3816
J = Indicates an estimated value
Analytical Batch
SL513
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
325
Accutest Laboratories
Client Sample ID: R WSF-l
Lab Sample ID: Fl 0823-l
•
Matrix: AQ -Ground Water
Report of Analysis
Date Sampled: 09/04/0 l
Date Received: 09/06/0 l
Percent Solids: n/a
Page l of l
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte
Barium
Beryllium
Lead
Manganese
Nickel
Result
254-:S
I.I ws--
24.3
90.1 S°
3.5 jl.J"
RL = Reporting Limit
RL
200
5.0
5.0
15
40
ID L = Instrument Detection Limit
IDL
0.94
0.22
1.2
0.26
0.80
Units DF Prep Analyzed By Method
ug/l 09/13/01 09/18/0l JK SW846 60IOB
ug/l 09/13/0l 09/18/01 JK SW846 6010B
ug/1 09/13/01 09/18/0l JK SW846 601GB
ug/l 09/13/0l 09/18/0 l JK SW846 60108
ug/l 09/13/0l 09/18/0l JK SW846 60108
~rv'C..
Io\ \ \;:,, •
U = Indicates a result < IDL
B = Indicates a result > = IDL but < RL
012
Accutest Laboratories • Report of Analysis Page 1 of l
Client Sample ID: RWSF-l
Lab Sample ID: Fll750-5
Matrix: AQ · Ground Water
Method: SW846 8260B
Project: GELS, Hendersonville, NC
File ID OF
Run #I HOl47l2.D l
Run #2
VOA TCL List
CAS No. Compound
7 l-43-2 Benzene
67-66-3 Chloroform
107-06-2 l,2-Dichloroethane
156,59-2 cis-l ,2-Dichloroethylene
l 56-60-5 · trans-l ,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-0 l-6 Trichloroethylene
75-0 l-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
17060-07-0 l ,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromotluorobenzene
ND = Not detected
RL = Reporting Limit
Analyzed
12/17/01
Result
ND
ND
ND
ND
ND
52.6
ND
ND
Run# 1
99%
101 %
100%
100%
E = Indicates value exceeds calibration range
By
NAF
RL
l.O
2.0
2.0
2.0
2.0
2.0
2.0
l.O
Run# 2
Date Sampled: 12/11/01
Date Received: 12/12/0 I
Percent Solids: n/a
Prep Date Prep Batch Analytical Batch
nia n/a VH469
Units Q
ug/l
ug/1
ug/l
ug_!!
ugll
ug/l
ug/1
ug/1
Limits
80-120%
80-120%
80-120%
80-120%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
016
Accutest Laboratories •
Report of Analysis Page l of l
Client Sample ID: RWSF-l
Lab Sample ID: Fl l 750-5
Matrix:
Method:
Project:
AQ -Ground Water
SW846 8270C SW846 35 l0C
GELS, Hendersonville, NC
File ID
L0l0044.D
DF Analyzed By
Run #l
Run #2
ABN TCL List
CAS No.
98-95-3
CAS No.
367-12-4.
4165-62-2
l l8-79-6
4 l 65-60-0
321-60-8
1718-51-0
Compound
Nitrobenzene
Surrogate Recoveries
2-Fluorophenol
Phenol-dS
2,4,6-Tribromophenol
Nitrobenzene-d5
2-Fluorobiphenyl
Terphenyl-dl4
ND = Not detected
RL = Reporting Limit
12/!7/0l ME
Result RL
ND 5.0
Run# 1 Run# 2
51 %
36%
87%
83%
76%
80%
E = Indicates value exceeds calibration range
Date Sampled: 12/l l/0l
Date Received: l 2/l 2/0 I
Percent Solids: n/a
Prep Date
!2/l4/0l
Units Q
ug/l
Limits
20-125%
l0-l25%
35-l40%
46-125%
46-l25%
49-l26%
Prep Batch
OP4380
J = Indicates an estimated value
Analytical Batch
SL570
025
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
029
Accutest Laboratories •
Client Sample ID: R WSF-l
Lab Sample ID: Fl l 750-5
Matrix: AQ -Ground Water
Report of Analysis
Date Sampled: l 2/ I l/O l
Date Received: 12/ l 2/0 I
Percent Solids: n/a
Page l of l
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units DF Prep Analyzed By Method Prep :Vlethod
Barium l53 -s::i;, 200 0.94 ug/1 12/14/01 12/l 7/0l OM SW846 60108 SW346 J0I0A
Beryllium 1.2 s-::f} 5.0 0.22 ug/1 l2/14/0I l2/17/0I OM SW846 60108 SW846 J0IOA
Lead l0.4 \J \ 5.0 l.2 ug/1 12/14/0l 12/17/0l DM SW846 60108 SW846 J0IOA
Manganese 71.8 ~). 15 0.26 ug/1 l2/14/0l 12/17/01 DM SW846 60108 SW846 J0I0A
Nickel 1.8 B-.)3, 40 0.80 ug/l 12/14/01 12/17/0l DM SW846 60108 SW846 J0IOA
0.ZG
RL ; Reponing Limit IJ ; Indicates a result < IDL
IDL ; Instrument Detection Limit B ; Indicates a result >; IDL but < RL
041
www.geotransi nc.colll
Dr. Gary Hi II
250 Old TyTy Road
Tifton, GA 31794-6607
Reference:
Dear Dr. Hill:
Groundwater Sampling Results
September 2000 to December 200 I
Geo Trans Project No, P82 l-lO I
@ OBO Holcolllb 13riclge Road
Builcl111g 100, Suite 190
Roswell, GA 30076
770-642-1 O(Hl FAX 770-642-ililOS
APR 1 5 2002
L ..
Per your request the results from the recovery and monitoring wells on your property are
provided, The groundwater was analyzed for seven target volatile organic compounds (VOCs),
one semi-volatile organic compound (SVOC), and five metals, All field and laboratory methods
utilized were approved by the U.S. Environmental Protection Agency (EPA). The results from
September 2000 until December 2001 for MW-64, MW-64A, MW-66 and RWSF-l(see Figure I)
are provided in the attached laboratory reports and are summarized in the attached tables,
EPA requires General Electric to sample the wells quarterly as part of a long-term
monitoring plan. The groundwater will continue to be sampled for seven VOCs, and five metals.
The one SYOC, nitrobenzene, has been removed from the quarterly sampling events with EPA
approval. It will be sampled only during the annual sampling events that occur in September of
every year. In the event that nitrobenzene is recovered during the annual sampling event it will be
placed back onto the list for quarterly sampling. We will report groundwater sampling results to
you as they become available. If you have any questions, please feel free to call me at (770) 642-
IOOO or Mr. Lee Humphrey at [phone],
cc, Giezelle Bennett (EPA)
Lee Humphrey (GELS)
David Mattison (NCDENR)
P:\GE\DOCS\RE.'\JDENl\llill Rcsuh, 1 l-Ol .wpJ
April 12. 2002
Sincerely,
~;,_ Ill'-! cu,ljt__/
Patricia Hermann
Project Scientist
P:\GE\rgvp\gis-rgvp\SFs11e.wor
-------r
,~ !
--~--_J
I
I
i
I -,----
' ,:xi:· i
I
/ t
L
/_ __ •-
I =
__ L_
I _I __ _
---/---
I
----~-
Expla11atio11
• Site monitor well
♦ Recovery well
' ' _J_ -
+ Sampled Residential well
G Piezometer
' ' ·:---._ ""--~----·---::::,, RWSF-4'-
-... -,_
-------',,'"-.. , MW-64A ::::----•
------.::::::--:::---!]q , ~--
----.:__------
---.< ..... ,_ =o ·--........:,-, ----,--------...... ,, ....... ,,
---------------Q----8 \ '<;_::....... -----~ ..... ~ .....
"~
-------
'/··□· / 1 -'
'
I I ' I I
I ---r--r----_,
~~==:=~-" 1-1 _1 I i n ~~· ----'' _,,,
TITLE:
Location of Shepherd Farm Subsite Features
LOCATION:
0 300
East Flat Rock, NC
600 t-----------------===--=~--~----1 ~GeoT ~:~:~ ::; FIGURE:
SCALE IN FEET z ,4 A TETRA 1ECH COllP~! I rans' Inc . .-,-,,-E--+-s,-,-,ie-.w-o,--
DATE 11/30/01
1
•
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results.
Remediation
Parameter Goal
voes (µg/L)
1,2-Dichloroethane
Benzene
Chloroform
cis-1,2-Dich\oroethenc
Tetrach\orocthene
trnns-1,2-Dichloroethene
Trlchloroethene
Vinyl chloride
SVOCs (µg/L)
Nitrobenzene
I\IETALS TOTAL (ftg/L)
Barium
Beryllium
Lead
M:mganese
Nickel
Notes:
U,NO -not detected
J -detected, estimated result
UJ • not detected, estimated result
D -dilution sample
E -exceed calibration limit
B -found in blank
70
70
2.8
10
2000
4
15
50
100
MW-64
Scp-00 Dcc-00 Mar-01 Jun-01 Scp-01 Dec-01
ND (2.0) ND (2.01 ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND(I.O) ND (1.0)
1.0 J ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2-0) ND (2.0) ND (2.0)
3.6 2.8 0.83 J 1.9 J s.o 3.0
ND (2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0) ND (1.0)
ND (5.0) ND (5.0) ND (5.5) ND (5.0) ND (5.0) ND (5.0)
37.9 B 53.0 J 20. l J 22.0 J 37.9 J 34.5 J
0.68 J 0.68 U 0.51 U 0.75 U 0.67 U 0.45)
1.5 J 12.7 3.4U l.3 u l.2 u 4.7U
8.4 J 27.7 2.7 UJ 2.7 U 3.4 UJ 7.0 J
5.4 lJ 0.8 lJ l.2 J 0.8 U 0.8 U 0.8 U
Balded values indicate detected concentrations greater than remediation goals.
Mar-02 Jun-02 Sep-02 Dec-02
•
Accutest LabLink@7822 09:.8-Oct-2000 .G Report of Analysis Page I of I
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
Project:
MW-64
F7H9-3
AQ -Ground Water
SW846 8260B
GELS, Hendersonville. NC
File ID
B002320.D
OF Analyzed By
Run #I
Run #2
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 1,2-Dichloroethane
156-59-2 cis-1,2-Dichloroethylene
156-60-5 trans-1,2-Dichloroethylene
127-18:4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Oibromofluoromethane
17060-07-0 l ,2-Dichloroethane-D4
2037-26-5 Toluene-DB
460-00-4 4-B ro mo fluorobenzene
ND = Not detected
RL = Reporting Limit
10/09/00 JG
Result
ND
1.0
ND
ND
ND
3.6
ND
ND
Run# I
93%
94%
109%
103%
E = Indicates value exceeds calibration range
RL
1.0
2.0
2.0
2.0
2.0
2.0
2.0
1.0
Run# 2
Date Sampled: 09/28/00
Date Received: 09/29/00
Percent Solids: n/a
Prep Date
n/a
Units Q
ug/1
ug/1 J
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
Limits
80-120%
69-128%
80-120%
80-120%
Prep Batch
n/a
Analytical Batch
VBH
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
Accutest Lablink@7822 09:18-Oct-2000 4j
Report of Analysis
Client Sample ID: MW-64
Lab Sample ID: F77 49-3
Matrix: AQ -Ground Water
Method: SW846 3510C/8270C
Project: GELS, Hendersonville, NC
File ID DF
Run #1 W002725.D 1
Run #2
ABN TCL List
CAS No. Compound
98-95-3 Nitrobenzene
CAS No. Surrogate Recoveries
367-12-4 2-Fluorophenol
4165-62-2 Phenol-d5
118-79-6 2. 4. 6-Tribromophenol
4165-60-0 Nitrobenzene-d5
321-60-8 2-Fluorobiphenyl
1718-51-0 Terphenyl-d14
ND = Not detected
RL = Reporting Limit
Analyzed
10/10/00
Result
ND
Run# 1
46%
29%
85%
77%
74%
91%
E = Indicates value exceeds calibration range
By
ME
RL
5.0
Run# 2
Page 1 of l
Date Sampled: 09/28/00
Date Received: 09/29/00
Percent Solids: n/a
Prep Date Prep Batch Analytical Batch
10/03/00 OP2129 SW165
Units Q
ug/1
Limits
21-100%
10-94%
10-123%
35-114%
43-116%
33-141%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
Accutest LabLink@7822 09:,8-Oct-2000
Client Sample ID:
Lab Sample ID:
Matrix:
MW-64
F7749-3
AQ -Ground Water
Report of Analysis •
Date Sampled: 09/28/00
Date Received: 09/29/00
Percent Solids: n/a
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL Units OF Prep Analyzed By Method
Barium 37.9 B 200 ug/1 1 10/04/00 10/06/00 JK SW846 60108
Beryllium 0.68 B · 5.0 ug/1 I 10/04/00 10/06/00 JK SW846 60108
Lead 1.5 B 5.0 ug/1 1 10/04/00 10/06/00 JK SW846 60108
Manganese 8.4 B 15.0 ug/1 1 10/04/00 10/06/00 JK SW846 60108
Nickel 5.4 B 40.0 ug/1 l 10/04/00 10/06/00 JK SW846 60108
RL = Reporting Limit
Page I of I
Report of Analysis Page 1 of 1
Client Sample ID: MW-64
Lab Sample ID: F8335-1 Date Sampled: 12/07 /00
Matrix: AQ -Ground Water Date Rccei vcd: 12/08/00
Method: SW846 8260B Percent Solids: n/a
Project: GELS, Hendersonville. NC
File ID DF
Run #1 C0001712.D I
Run #2
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107,06-2 1, 2-Dichloroethane
156-59-2 cis-1,2-Dichloroethylene
156-60-5 trans-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Dibromot1uoromethane
17060-07-0 1,2-Dichloroethane-D4
2037-26-5 Toluene-OS
460-00-4 4-B romo 11 uo robenzene
ND = Not detected
RL = Reponing Limit
Analyzed By Prep Date
12/12/00 JG n/a
Result RL Units Q
ND 1.0 ug/1
ND 2.0 ug/l
ND 2.0 ug/1
ND 2.0 ug/1
ND 2.0 ug/1
2.8 2.0 ug/l
ND 2.0 ug/1
ND 1.0 ug/1
Run# l Run# 2 Limits
98% 80-120%
104% 69-128%
99% 80-120%
100% 80-120%
~J}v'V(_
1\'?:~·\\c,
Prep Batch Analytical Batch
n/a VC78
J = [ndicates an estimated value
E = [ndicates value exceeds calibration range
B = [ndicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
• 0
Report of Analysis Page 1 of 1
Client Sample ID: MW-64
Lab Sample ID: F8335-l
Matrix:
Method:
Project:
AQ -Ground Water
SW846 8270C SW846 35I0C
GELS, Hendersonville, NC
File ID
W003361.D
DF Analyzed By
Run #l
Run #2
ABN TCL List
CAS No.
98-95-3
CAS No.
367-12-4
4165-62-2
l l 8-79-6
4165-60-0
321-60-8
1718-51-0
Compound
Nitro benzene
Surrogate Recoveries
2-Fluorophenol
Phenol-dS
2,4,6-Tribromophenol
Nitrobenzene-dS
2-Fluorobiphenyl
Terphenyl-dl4
ND = Not detected
RL = Reporting Limit
12/15/00 ~!E
Result RL
ND 5.0
Run# 1 Run#2
43%
26%
83%
86%
80%
95%
E = Indicates value exceeds calibration range
Date Sampled:
Date Received:
Percent Solids:
12/07 /00
12/08/00
n/a
Prep Date
12/l2/00
Prep Batch
OP2420
Cnits Q
ug/l
Limits
21-100%
10-94%
10-123 %
35-114%
43-116%
33-141 %
Analytical Batch
SWl99
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidenceiJf a compound -··•· .......
Report of Analysis Page l of 1
Client Sample ID: MW-64
Lab Sample ID: F8335-l
Matrix: AQ -Ground Water
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL Units DF
Barium 53 o B"S 200 ug/l
Beryllium 0.68 B-J 5.0 ug/1
Lead 12.7 5.0 ug/1
Manganese 27.7 15.0 ug/1
Nickel 0.80 U 40.0 ug/1
Prep
12/J 1/00
12/11/00
12/11/00
12/1\/00
12/11/00
Date Sampled: 12/07 /00
Date Received: \2/08/00
Percent Solids: n/a
Analyzed By Method
12/13/00 JK SW846 60108
12/13/00 JK SW846 60108
12/13/00 JK SW846 60!08
12/13/00 JK SW846 60l0B
12/13/00 JK SW846 60108
. \ \J . ¼ c\,,_: ~ -b \0 \ 0., ~ c. .. ,:::YAA v~-r\o:ria'"'
~~0lt:, ,,:, L S ~
RL = Reporting Limit
• Report of Analysis Pagelofl
Client Sample ID: MW-64
Lab Sample ID: F9 l 96-5
Matrix:
Method:
AQ -Ground Water
SW846 8260B
Project: GELS, Hendersonville, NC
Run #1
Run #2
File ID
C0003076.D
DF
VO.\ TCL List
CAS No, Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 1,2-Dichloroethane
156-.59-2 cis-1,2-Dichloroethylene
156-60-5' trans-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
17060-07-0 l ,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromotluorobenzene
ND = Not detected
RL = Reporting Limit
Analyzed By
03/16/01 JG
Result RL
ND l.O
ND 2.0
ND 2.0
ND 2.0
ND 2.0
0.83 2.0
ND 2.0
ND 1.0
Run# l Run# 2
94%
99%.
105%
100%
E = Indicates value exceeds calibration range
Date Sampled: 03/14/01
Date Received: 03/15/01
Percent Solids: n/a
Prep Date
n/a
Units Q
ug/1
ug/1
ug/1
ug/1
ug/l
ug/1 J
ug/l
ug/1
Limits
80-120%
69-128%
80-120%
80-120%
__ .. ..--~
i,,r,---,, ·'..,~::.:
Prep Batch
n/a
J = Indicates an estimated value
Analytical Batch
VC145
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
38
• Report of Analysis Page I of I
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
Project:
MW-64
F9 l 96-5
AQ -Ground Water
SW846 8270C SW846 351 OC
GELS, Hendersonville, NC
File ID
L006827.D
OF Analyzed By
Run #I
Run #2
ABNTCL List
CAS No.
98-95-3
CAS No.
367-i2-4 ·
4165-62-2
118-79-6
4165-60-0
321-60-8
1718-51-0
Compound
Nitro benzene
Surrogate Recoveries
2-Fluorophenol
Phenol-dS
2 ,4. 6-Tribromophenol
Nitrobenzene-dS
2-Fluorobiphenyl
Terphenyl-dl4
ND = Not detected
RL = Reporting Limit
03/20/01 ~IE
Result RL
ND 5.5
Run# l Run# 2
48%
32%
90%
76%
71%
94%
E = Indicates value exceeds calibration range
Date Sampled:
Date Received:
Percent Solids:
03/14/01
03/15/01
n/a
Prep Date
03/ 19/01
Prep Batch
OP2873
Units Q
ug/l
Limits
21-100%
10-94%
10-123%
35-114%
43-116%
33-141 %
,.,.,....
:'_,,,.,:'1· \, -'1':.___
J = Indicates an estimated value
Analytical Batch
SL404
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
zo1
Client Sample ID: MW-64
Lab Sample ID: F9 l 96-5
Matrix: AQ -Ground Water
Report of Analysis Page 1 of 1
Date Sampled: 03/14/01
Date Received: 03/15/01
Percent Solids: n/a
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units OF Prep Analyzed By Method
Barium 20.1,,s' :J 200 0,94 ug/l 03/20/0 l 03/27 /0 l JK SW846 60108
Beryllium 0.5L!f' L" 5.0 0.22 ug/1 03/20/01 03/27 /0 l JK SW846 60IOB
Lead 3.4.B' . , 5.0 1.2 ug/1 03/20/0 l 03/27/01 JK SW846 60IOB ' ·, <..'. Jl5 0.26 03/27 /0 l Manganese 2.7.B ug/1 03/20/01 JK SW846 60l0B
Nickel 1.2 ,( _., 40 0.80 ug/1 03/20/01 03/27 /0 l JK SW846 60l0B
RL = Reporting Limit U = Indicates a result < IDL
ID L = Instrument Detection Limit B = Indicates a result > = IDL but < RL
Accutest Laboratories • Report of Analysis Page 1 of l
Client Sample ID: MW-64
Lab Sample ID: F9887-l
Matrix: AQ -Ground Water
Method: SW846 8260B
Project: GELS, Hendersonville, NC
File ID DF
Run #1 H012170.D I
Run #2
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 1,2-Dichloroethane
156-59-2 cis-1,2-Dichloroethylene
156-60-5 trans-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Dibromotluoromethane
17060-07-0 1,2-Dichloroethane-D4
2037-26-5 Toluene-DB
460-00-4 4-Bromotluorobenzene
ND = Not detected
RL = Reporting Limit
Analyzed
06/13/01
Result
ND
ND
ND
ND
ND
l.9
ND
ND
Run# I
104%
117%
94%
98%
E = Indicates value exceeds calibration range
Date Sampled: 06/05/0 l
Date Received: 06/06/01
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
NAF n/a n/a VH340
RL Units Q
l.O ug/1
2.0 ug/1
2.0 ug/1
2.0 ug/1
2.0 ug/1
2.0 ug/1 J
2.0 ug/1
l.O ug/1
Run# 2 Limits
80-120%
80-120%
80-120%
80-120% 2·-·
)',r,, ,..:_
. \--. -.-. \:: \
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
Accutest Laboratories • Report of Analysis Page 1 of 1
Client Sample ID: MW-64
Lab Sample ID: F9887-1
Matrix: AQ -Ground Water
Method:
Project:
SW846 8270C SW846 35 l0C
GELS, Hendersonville, NC
Run #I
Run #2
File ID
W005366.D
ABN TCL List
CAS No. Compound
98-95-3 Nitrobenzene
OF Analyzed By
06/11/01 ME
Result RL
ND 5.0
Date Sampled: 06/05/0 l
Date Received: 06/06/0 I
Percent Solids: n/a
Prep Date
06/07 /0 I
Units Q
ug/1
Prep Batch
OP3268
Analytical Batch
SW296
CAS No.
367°12-4.
4165-62-2
118-79-6
4165-60-0
321-60-8
1718-51-0
Surrogate Recoveries Run# 1 Run# 2 Limits
2-Fluorophenol
Phenol-d5
2.4,6-Tribromophenol
N itrobenzene-d5
2-Fluorobiphenyl
Terphenyl-dl4
ND = Not detected
RL = Reporting Limit
52%
35%
96%
95%
89%
90%
E = Indicates value exceeds calibration range
20-125%
10-125%
35-140%
46-125%
46-125%
49-126%
------
( -.j'..--" \L--. ,;..;,,--\ . , -,:'(-, \ ~ ·, ✓
_,,1_ ·., _.,,,.
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
::, ·; c-
••J ,...., ,_)
Accutest Laboratories
Client Sample ID: MW-64
Lab Sample ID: F9887-l
•
Matrix: AQ -Ground Water
Report of Analysis
Date Sampled: 06/05/0 l
Date Received: 06/06/0 l
Percent Solids: n/a
Pagt:: l of l
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units DF Prep Analyzed By Method
Barium 22.0 B'·T 200 0.94 ug/l 06/07 /0 l 06/08/0 l JK SW846 60108
Beryllium 0.75.J{U 5.0 0.22 ug/1 06/07 /0 l 06/08/0 l JK SW846 60108
Lead l.3 B ,J 5.0 l.2 ug/l 06/07 /0 l 06/08/0 l JK SW846 6010B
Manganese 2.7 B \.J 15 0.26 ug/1 06/07 /0 l 06/08/0 l JK SW846 60108
Nickel 0.80 U 40 0.80 ug/l 06/07 /0 l 06/08/01 JK SW846 60108
RL = Reporting Limit
IDL = Instrument Detection Limit
U = Indicates a result < ID L ': -~ ,-
B = Indicates a result > = IDL tmt'"<'.RL
Accutest Laboratories • Report of Analysis Page t oft
Client Sample ID: MW-64
Lab Sample ID: FI0823-8
i\ilatrix:
Method:
AQ -Ground Water
SW846 82608
Project: GELS, Hendersonville, NC
Run #I
Run,#2
File ID
C0005639.D
DF
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 I, 2-Dichloroethane
156-_59-2 cis-1,2-Dichloroethylene
156-60-5' trans-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CAS No. Surrogate Recoveries
I 868-53-7 Dibromofluoromethane
17060-07-0 I, 2-Dichloroethane-D4
2037-26-5 Toluene-DB
460-00-4 4-Bromofluorobenzene
ND = Not detected
RL = Reporting Limit
Analyzed
09/13/01
Result
ND
ND
ND
ND
ND
5.0
ND
ND
Run# I
104%
115%
100%
96%
E = Indicates value exceeds calibration range
By
JG
RL
1.0
2.0
2.0
2.0
2.0
2.0
2.0
LO
Run# 2
Date Sampled: 09/05/0 I
Date Received: 09/06/0 I
Percent Solids: n/a
Prep Date
n/a
Units Q
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
Limits
80-120%
80-120%
80-120%
80-120%
Prep Batch
n/a
Analvtical Batch
~7-• '.J 1...-' _,, -~;;> r:._. -
-.;)-r""',· .... ~
' ,
;...; '=. -..; \_
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compo1,d() 3
Accutest Laboratories • Report of Analysis Page l of 1
Client Sample ID: MW-64
Lab Sample ID: F10823-8
Matrix:
Method:
Project:
AQ -Ground Water
SW846 8270C SW846 35 I0C
GELS, Hendersonville, NC
File ID
L008971.D
OF
1
Analyzed By
Run #I
Run #2
ABN TCL List
CAS No.
98-95-3
CAS No.
367-12-4
4165-62-2
118-79-6
4165-60-0
321-60-8
1718-51-0
Compound
Nitrobenzene
Surrogate Recoveries
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
Nitrobenzene-d5
2-Fluorobiphenyl
Terphenyl-dl4
ND = Not detected
RL = Reporting Limit
09/13/01 ME
Result RL
ND 5.0
Run# l Run# 2
45%
30%
83%
70%
70%
91 %
E = Indicates value exceeds calibration range
Date Sampled: 09/05/0 I
Date Received: 09/06/0 I
Percent Solids: n/a
Prep Date
09/09/0 I
Units Q
ug/1
Limits
20-125%
10-125%
35-140%
46-125%
46-125%
49-126%
Prep Batch
OP3816
J = Indicates an estimated value
Analytical Batch
SL513
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
345.
Accutest Laboratories • Report of Analysis Page 1 of l
Client Sample ID: M W-64
Lab Sample ID: Fl 0823-8
i\latrix: AQ -Ground Water
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units OF
Barium 3 7 . 9 JY"S' 2 00 0.94 ug/1
Beryllium 0.67,lYI.) 5.0 0.22 ug/l
Lead l.2 U 5.0 l.2 ug/1
Manganese 3.4 IV'~ 15 0.26 ug/l
Nickel 0.80 U 40 0.80 ug/1
·'\?f1Y-YY<'.'..
1c.c\ ·,; jc: I
RL = Reporting Limit
IDL = Instrument Detection Limit
Date Sampled: 09/05/0 I
Date Received: 09/06/0 l
Percent Solids: n/a
Prep Analyzed By Method
09/13/01 09/19/0l JK SW846 60108
09/13/0 l 09/19/0 l JK SW846 60108
09/13/0l 09/19/01 JK SW846 60!0B
09/13/0 l 09/19/0 l JK SW846 6010B
09/13/0l 09/19/0l JK SW846 6010B
U = Indicates a result < IDL
B = Indicates a result > = IDL but < RLQ 3 2
Accutest Laboratories • Report of Analysis Page l of l
Client Sample ID: MW-64
Lab Sample ID: Fl l 750-10
Matrix: AQ · Ground Water
Method: SW846 8260B
Project: GELS, Hendersonville, NC
File ID OF
Run#l H014716.D l
Run #2
VOA TCL List
CAS No. Compound
7 l-43-2 Benzene
67-66-3 Chloroform
107-06-2 l ,2-Dichloroethane
156-59-2 cis-l ,2-Dichloroethylene
156:60-5. trans-l ,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-0 l-6 Trichloroethylene
75-0 l-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Dibromot1uoromethane
l 7060-07-0 l ,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromofluorobenzene
ND = Not detected
RL = Reporting Limit
Analyzed
12/l7/0I
Result
ND
ND
ND
ND
ND
3.0
ND
ND
Run# I
100%
105%
100%
100%
E = Indicates value exceeds calibration range
By
NAF
RL
l.O
2.0
2.0
2.0
2.0
2.0
2.0
l.O
Run# 2
Date Sampled: 12/l l/0l
Date Received: 12/12/01
Percent Solids: n/a
Prep Date Prep Batch Analytical Batch
n/a n/a VH469
units Q
ug/1
ug/l
ug/1
ug/1
ug/l
ug/1
ug/l
ug/1
Limits
80-120%
80-120%
80-120%
80-120%
J = Indic:ites an estimated value
B = indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
021
Accutest Laboratories • Report of Analysis Page 1 of 1
Client Sample ID: MW-64
Lab Sample ID: F\1750-10
Matrix: AQ -Ground Water
Method: SW846 8270C SW846 3510C
Project: GELS, Hendersonville, NC
File ID OF
Run #1 L0I0050.D I
Run #2
ABN TCL List
CAS No, Compound
98-95-3 Nitro benzene
CAS No. Surrogate Recoveries
367-12-4. · 2-Fluorophenol
4165-62-2 Phenol-d5
118-79-6 2,4,6-Tribromophenol
4165-60-0 Nitrobenzene-d5
321-60-8 2-Fluorobiphenyl
1718-51-0 Terphenyl-dl4
ND ; Not detected
RL ; Reponing Limit
Analyzed
12/17/01
Result
ND
Run# 1
42%
28%
57%
58%
53%
58%
E = Indicates value exceeds calibration range
By
ME
RL
5.0
Run# 2
Date Sampled: 12/11/01
Date Received: 12/12/0 I
Percent Solids: n/a
Prep Date Prep Batch Analytical Batch
12/14/01 OP4380 SL570
Units Q
ug/1
Limits
20-125%
10-125 %
35-140%
46-125%
46-125 %
49-126%
J ; Indicates an estimated value
B ; Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
034
Accutest Laboratories •
Client Sample ID: MW-64
Lab Sample ID: Fl 1750-lO
Matrix: AQ -Ground Water
Report of Analysis
Date Sampled: 12/11/01
Date Received: 12/12/0l
Percent Solids: n/a
Page l of I
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units DF Prep Analyzed By Method Prep Method
Barium 34.5 8'31 200 0.94 ug/1 12/14/01 12/17/01 DM SW846 60l08 SW846 J0l0A
Beryllium 0.45 8-.;} 5.0 0.22 ug/1 12/14/01 12/17/01 DM SW846 60108 SW846 J0\0A
Lead 4.7'B.. \) \ 5.0 1.2 ug/1 12/14/01 [2/17/01 DM SW846 60108 SW846 J0lDA
Manganese 7.0B..-:i). 15 0.26 ug/l 12/14/01 12/17/01 DM SW846 60108 SW846 J0\0A
Nickel 0.80 U 40 0.80 ug/1 12/14/01 12/17/01 DM SW846 60108 SW846 J0l0A
I I I I : I
I i L{1 CJ--
1
RL = Reponing Limit U = Indicates a result < IDL
IDL = Instrument Detection Limit B = Indicates a result > = IDL bu1 < RL
045
Table 1. Shepherd Farm Subsite -Performance Well Analytical Results. (continued)
Remediation MW-64A
Parameter Goal Sep-00 Dec-00 Mar-01 Jun-OJ Sep-OJ Dec-OJ
voes (µg/L)
1,2-Dichloroethane ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
Benzene ND (LO) ND (LO) ND (LO) ND (1.0) ND (LO) ND (LO)
Chloroform ND (2.0) ND (2.0) ND (2.0) 0.68 J 0.68 J ND (2.0)
cis-1,2-Dichlorocthcnc 70 ND (2.0) ND (2.0) ND(2.0) ND (2.0) ND (2.0) ND (2.0)
Tctrachlorocthcne 50.2 46.7 43.1 41.8 42.8 41.8
trans-1,2-Dich!oroethene 70 ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
Trichlorocthenc 2.8 ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0)
Vinyl chloride ND (LO) ND (LO) ND (LO) ND (LO) ND (LO) ND (LO)
SVOCs (µg/L)
Nitro benzene 10 ND (5.0) ND (5.0) ND (5.0) ND (5.0) ND (5.0) ND (5.0)
METALS TOTAL (µg/L)
Barium 2000 34.0 J 33.6 J 36.0 J 32.7 J 29.7 J 30.2 J
Beryllium 4 0.79 U 0.86 UJ 0.76 U 0.83 U 0.6 U 0.22 U
Lead I 5 1tc§:y7 1.7 UJ 2.5 U 1.4 U L2 J 4.4 U
Manganese 50 90.7 7 76.9 J 92.4 J 70.8 51.4 J 50.4
Nickel 100 L9 U 0.8 UJ 0.97 J 0.8 U 0.8 U 0.8 U
Notes: Balded values indicate detected concentrations greater than remediation goals.
U,ND -not detected
J -detected, estimated result
UJ -not detected, estimated result
D -dilution sample
E -exceed calibration limit
B -found In blank
Mar-02 Jun-02 Sep-02 Dec-02
•
~~ • ~ACCUTEST.
Report of Analysis Pagelofl
Client Sample ID: MW-64A
Lab Sample ID: F7734-3
Matrix:
Method:
AQ -Ground Water
SW846 8260B
Projeet: GELS, Hendersonville, NC
Run #l
Run #2
File ID
B002233.D
DF
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 C1loroform
i0/-06-2 : . .:-Dic:1ioroethane
156-59-2 . cis-1,2-Dichloroethylene
156-60-5 trans-l .2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-0 l-6 Tr:chloroethylene
75-0 l-4 Vinyl chloride
CAS No. Surrogate Recoveries
l 868-53-7 Dibrcmor1uoromethane
l 7060-07-0 l ,2-Dichloroethane-D4
2037-26-5 Toiuene-D8
460-00-4 4-Bromo tluorobenzeae
ND ; Not detected
RL ; Reporting Limit
Analyzed
10/05/00
Result
ND
ND
ND
ND
ND
50.2
ND
ND
Run# I
93%
102%
114%
118%
E ::::: Indicates value exceeds calibration range
By
JG
RL
1.0
2.0
2.0
2.0
2.0
2.0
2.0
1.0
Date Sampled: 09/27 /00
Date Reeeived: 09/28/00
Percent Solids: n/a
Prep Date
n/a
Units Q
ug/1
ug/l
ug1!
ug/1
ug/1
ug/l
ug/l
ug/1
Prep Batch
n/a
Analytical Batch
VB71
Run#2 Limits
80-120%
69-128%
80-120%
80-120%
J ; Indicates an estimated value
B ; Indicates analyte found in associated method blank
N ; Indicates presumptive evidence of a compound Q 15
Florida • 4405 Vineland Road • Su1!e C-15 • Orlando. FL 32811 • tel: -l07-425-6700 • :ax: JQ7-425-0707 • http://wwwaccutest.com
~~ • gACCUTEST.
Client Sample ID:
Lab Sample ID:
Matrix:
MW-64A
F7734-3
AQ -Ground Water
Report of Analysis
Method:
Project:
SW846 35 l0C/8270C
GELS, Hendersonville, NC
Date Sampled: 09/27 /00
Date Received: 09/28/00
Percent Solids: n/a
Run #l
Run #2
File ID
W002698.D
DF
ABN TCL List
CAS No.
98-95-3
C.-\S No.
367-l2-4
4 l65-62-2
118-79-6
4165-60-0
32 l-60-8
l7l8-5l-0
Compound
Nitrobenzene
Surrogate Recoveries
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
>litrobenzene-d5
2-Fluorobiphenyl
Terphenyl-dl4
Analyzed By
l0/09/00 ME
Result RL
ND 5.0
Run# 1 Run# 2
49%
30%
86%
87%
85%
91 %
Prep Date
l0/03/00
Units Q
ug/1
Limits
21-100%
10-94%
l0-123%
35-ll4%
43-l l6%
33-l4l %
Prep Batch
OP2129
J = Indicates an estimated value
Page l of l
Analytical Batch
SWl64
ND = Not detected
RL = Reponing Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound C 3 {)
Fluri1la • 4405 1/ineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com n-'I'?
~f!f •
~ACCUTEST.
Client Sample ID: MW-64A
Lab Sample ID: F7734-3
Matrix: AQ -Ground Water
Report of Analysis
Date Sampled: 09127100
Date Received: 09/28100
Percent Solids: n/a
Project: GELS, Hendersonville, NC
:\1etals Analysis
Analyte Result RL
Barium
Beryllium
Lead
Nickel
34.0 R_) l.,, 200
0.79'8. \) I 5.0
1.2 U 5.0
t.91i.. VI 40.0
RL = Reporting Limit
Units
ug/1
ug/l
ug!1
ug/1
DF Prep Analyzed By Method
09129/00 l0/02100 JK SW846 6010B
09129100 10102100 JK SW846 6010B
09129100 l0/02100 JK SW846 6010B
09129/00 10102/00 JK SW846 60!0B
Florida • 4405 Vi11eland Road • Suite C-15 • Orlando. FL 32811 • tel: [phone] • fax: [phone] • nno://www accutest.com
Page l oi l
C44
•
Report of Analysis Page 1 of 1
Client Sample ID: MW-64A
Lab Sample ID: F8302-3
l\'latrix: AQ -Ground Water
Method: SW846 82608
Project: GELS, Hendersonville, NC
File ID DF
Run #I C000l614.D I
Run #2
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chlorofom1
107-06-2 I , 2-Dichloroethane
156-59-2 cis-1,2-Dichlorocthylene
156-60-5 trans-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Di bro mo fl uoromethane
17060-07-0 1,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromofluorobenzene
ND = Not detected
RL = Reporting Limit
Analyzed
12/07 /00
Result
ND
ND
ND
ND
ND
46:7
ND
ND
Run# I
97%
101%
104%
100%
E :;;::; Indicates value exceeds calibration range
Date Sampled: 12/05/00
Date Received: 12/06/00
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
JG n/a n/a VC73
RL Units Q
1.0 ug/1
2.0 ug/1
2.0 ug/1
2.0 ug/1
2.0 ug/l
2.0 ug/1
2.0 ug/1
1.0 ug/l
Run# 2 Limits
80-120%
69-128%
80-120%
80-120%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
,,-.:1•-, •u"--t,...,,
Report of Analysis Page 1 of 1
Client Sample ID: MW-64A
Lab Sample ID: F8302-3
Matrix: AQ -Ground Water
Method:
Project:
SW846 8270C SW846 35 lOC
GELS, Hendersonville, NC
Run #1
Run #2
File ID
W003269.D
ABN TCL List
CAS No, Compound
Nitro benzene
DF Analyzed By
12/08/00 ME
Result RL
ND 5.0
Date Sampled: 12/05/00
Date Received: 12/06/00
Percent Solids: n/a
Prep Date
12/07 /00
Units Q
ug/1
Prep Batch
OP2404
Analytical Batch
SW\95
98-95-3
CAS No.
367-12-4
4165-62-2
118-79-6
4165-60-0
321-60-8
1718-51-0
Surrogate Recoveries Run# I Run# 2 Limits
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
Nitrobenzene-d5
2-Fluorobiphenyl
Terphenyl-dl4
ND = Not detected
RL = Reporting Limit
41%
25%
71 %
69%
66%
87%
E = Indicates value exceeds calibration range
21-100%
10-94%
10-123%
35-114%
43-116%
33-141 %
J = lndicatcs an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound~ c:-1.~-t ~
IWll'IAQ • ~LI
~ACCUTEST.
Report of Analysis
Client Sample ID: MW-64A
Lab Sample ID: F8302-3
~latrix: AQ -Ground Water
Date Sampled: I 2/05/00
Date Received: 12/06/00
Percent Solids: n/a
Project:
Metals Analysis
Analytc
Barium
Beryllium
Lead
Manganese
Nickel
GELS, Hendersonville, NC
Result RL Units DF Prep Analyzed lly Method
33.6 I/J' 200 ug/1 12/07/00 12/14/00 JK SW846 60108
o.s6 .B v-:i' 5.o ug/1 12/07/00 12/14/00 JK SW846 60108
1.1 e w5.0 ug/l 12/07/00 12/14/00 JK SW846 6010B
76.9 ::r 15.0 ug/1 12/07 /00 12/14/00 JK SW846 601013
0.80 UT 40.0 ug/1 12/07 /00 12/14/00 JK SW84660108
_j ':::, cv,, '(' \_1._ S i"\ c I: (' YD f <.:. r' l f •' e.:3 c.-v' -'1..L\.
~\"' r be-Sor-,cJ cU \~~C•'I 7 IC C'lt 2,.J.4.
rns\M'>P Ye..C' \o~
c\,..i((\ \ C.C,.:UL \<YV 7 Z..o7c
\
RL = Reporting Limit
Fl .. rida.• ,!<.05 1/irie12~,,: Road • Suile C· i5 • Orl,mdo, Fl 32311 • 1el: .lQ? .. \25-6700 • :a,: ,\Q7 .. t25-(,m7 • 11110://www;1ccu1est.com
Page 1 of l
•
Report of Analysis Page I of I
Client Sample ID: MW-64A
Lab Sample ID: F9196-4 Date Sampled: 03/14/0 I
Matrix: AQ -Ground Water Date Received: 03/15/01
Method: SW846 8260B Percent Solids: n/a
Project: GELS, Hendersonville, NC
File ID DF
Run #I C0003075.D I
Run #2
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 1,2-Dichloroethane
156-59-2 cis-1,2-Dichloroethylene
156-60-5 trans-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CASNo. Surrogate Recoveries
1868-53-7 Dibromol1uoromethane
17060-07-0 1,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromotluorobenzene
ND = Not detected
RL = Reporting Limit
Analyzed By Prep Date Prep Batch Analytical Batch
03/16/01 JG n/a n/a VCl45
Result RL Units Q
·.NDt ·•• 1.0 ug/1
ND/ 2.0 ug/1
N_D 2.0 ug/1
ND 2.0 ug/1
ND 2.0 ug/1
4'.U. 2.0 ug/1 Nb< .. · 2.0 ug/1 ND 1.0 ug/1
Run# 1 Run#2 Limits
96%-i 80-120%
100% 69-128%
106% 80-120%
100%. 80-120%
,-·~\
. \ (/r-y·""\ '· \ ... :
J = Indicates an estimated value
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
34
•
Report of Analysis Page 1 of 1
Client Sample ID: MW-64A
Lab Sample ID: F9196-4
Matrix: AQ -Ground Water
Method: SW846 8270C SW846 35 I0C
Project: GELS, Hendersonville, NC
File ID DF
Run #1 L006824.D 1
Run #2
ABN TCL List
CAS No. Compound
98-95-3 Nitrobenzene
CAS No. Surrogate Recoveries
367-12-4 2-Fluorophenol
4165-62-2 Phenol-d5
118-79-6 2,4,6-Tribromophenol
4165-60-0 Nitrobenzene-d5
321-60-8 2-Fluorobiphenyl
1718-51-0 Terphenyl-dl4
ND = Not detected
RL = Reporting Limit
Analyzed
03/20/01
Result
ND
Run# I
42%
27%
81%
68%
64%
88%
E = indicates value exceeds calibration range
Date Sampled: 03/14/01
Date Received: 03/15/01
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
ME 03/19/01 OP2873 SL404
RL Units Q
5.0 ug/1
Run#2 Limits
21-100%
10-94%
10-123%
35-114%
43-116%
33-141 %
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evid1.c{)~a compound
•
Client Sample ID: MW-64A
Lab Sample ID: F9196-4
Matrix: AQ -Ground Water
Report of Analysis
Date Sampled: 03/14/01
Date Received: 03/15/01
Percent Solids: n/a
Page 1 of 1
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units DF Prep Analyzed By Method
Barium 36.0)Y -T 200 0,94 ug/1 03/20/01 03/27 /0 I JK SW846 60I08
Beryllium o76.ir"'c•5.o 0.22 ug/1 03/20/0 I 03/27/01 JK SW846 60I08
Lead 25,!Y' u 5.0 1.2 ug/1 1 03/20/01 03/27 /01 JK SW846 60108
Manganese 92:4 <·'S'. 15 0.26 ug/1 1 03/20/01 03/27 /01 JK SW846 60108
Nickel 0.97,K:_f"40 0.80 ug/1 1 03/20/01 03/27 /0 I JK SW846 60I08
~ C, . i:,"(>\ \·-
A\ -z.s l--::.1
RL = Reporting Limit U = Indicates a result < lDL
lDL = Instrument Detection Limit B = Indicates a result > = lDL but < RL
Accutest Laboratories •
Report of Analysis Page I of I
Client Sample ID: MW-64A
Lab Sample ID: F9887-2
Matrix:
Method:
AQ -Ground Water
SW846 82608
Project: GELS, Hendersonville, NC
Run #I
Run #2
File ID
H012196.D
DF
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 1,2-Dichloroethane
!56'59-2 cis-1,2-Dichloroethylene
156-60-5 trans-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Dibromot1uoromethane
17060-07-0 l ,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromot1uorobenzene
ND = Not detected
RL = Reporting Limit
Analyzed
06/15/0 I
Result
ND
0:68
ND
ND
ND
41 :8
ND
ND
Run# 1
101%
·IOI%
9_6%
101%
E = Indicates value exceeds calibration range
By
NAF
RL
1.0
2.0
2.0
2.0
2.0
2.0
2.0
1.0
Date Sampled: 06/05/0 I
Date Received: 06/06/0 I
Percent Solids: n/a
Prep Date
n/a
Units Q
ug/1
ug/1 J
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
Prep Batch
n/a
Analytical Batch
VH342
Run# 2 Limits
80-120%
80-120%
80-120%
80-120%
.,-----, c•/ -~rrv·1 r,.:_
,0 \ ~-1 \.;;cl
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
Accutest Laboratories •
Report of Analysis Page I of l
Client Sample ID: MW-64A
Lab Sample ID: F9887-2
Matrix: AQ -Ground Water
Method: SW846 8270C SW846 35IOC
Project: GELS, Hendersonville, NC
File ID DF
Run #1 W005367.D I
Run #2
ABNTCL List
CAS No. Compound
98-95-3 Nitrobenzene
CAS No. Surrogate Recoveries
367-12-4 2-Fluorophenol
4165-62-2 Phenol-d5
118-79-6 2,4,6-Tribromophenol
4165-60-0 Nitrobenzene-d5
321-60-8 2-Fluorobiphenyl
1718-51-0 Terphenyl-dl4
ND = Not detected
RL = Reporting Limit
Analyzed
06/11/01
Result
ND
Run# 1
49%
31 %
94%
83%
79%
96%
E = Indicates value exceeds calibration range
Date Sampled: 06/05/01
Date Received: 06/06/0 I
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
ME 06/07 /0 l OP3268 SW296
RL Units Q
5.0 ug/1
Run# 2 Limits
20-125%
10-125%
35-140%
46-125%
46-125%
49-126%
,,...--
/ \'..,-(S:'.c
/'.;'l'i"\..' ·\·'·;\
v'· \'', '-' ,A~ ,·
· J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
,, ... " .<.·:~~
Accutest Laboratories •
Client Sample ID:
Lab Sample ID:
Matrix:
MW-64A
F9887-2
AQ -Ground Water
Report of Analysis
Date Sampled: 06/05/0 l
Date Received: 06/06/0 l
Percent Solids: n/a
Page l of l
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units DF Prep Analyzed By Method
Barium ·32fir~ 200 0.94 ug/1 06/07 /01 06/08/01 JK SW846 60108
Beryllium 0.83;/(\) 5.0 0.22 ug/l 06/07/01 06/08/0 l JK SW846 60!08
Lead .1.4.B):0 r 5.0 1.2 ug/l 06/07 /01 06/08/0 I JK SW846 60l0B
Manganese 7o,3L < 15 0.26 ug/l 06/07 /01 06/08/01 JK SW846 60108
Nickel 080U ·•:':: 40 0.80 ug/l 06/07 JO l 06/08/01 JK SW846 60108
RL = Reponing Limit U = Indicates a result < IDL
IDL = Instrument Detection Limit B = lndicares a result > = IDL bur < RL
--~, -.J('• u ._; 0
Accutest Laboratories •
Report of Analysis Page I of I
Client Sample ID: MW-64A
Lab Sample ID: FI0823-2
Matrix: AQ -Ground Water
Method: SW846 82608
Project: GELS, Hendersonville, NC
File ID DF
Run #I C0005616.D I
Run #2
VOA TCL List
CAS No. Compound
71-43-2 Benzene
67-66-3 Chloroform
107-06-2 1,2-Dichloroethane
156-59-2 cis-1,2-Dichloroethylene
156-60-5 trans-1,2-Dichloroethylene
127-18-4 Tetrachloroethylene
79-01-6 Trichloroethylene
75-01-4 Vinyl chloride
CAS No. Surrogate Recoveries
1868-53-7 Dibromotluoromethane
17060-07-0 1,2-Dichloroethane-D4
2037-26-5 Toluene-OS
460-00-4 4-Bromotluorobenzene
ND = Not detected
RL = Reporting Limit
Analyzed
09/12/01
Result
ND
0,68
ND
ND
ND
42.8
ND
ND
Run# I
10(%
114%
98%
96%
E = Indicates value exceeds calibration range
Date Sampled: 09/04/01
Date Received: 09/06/01
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
JG n/a n/a VC271
RL Units Q
1.0 ug/1
2.0 ug/1 J
2.0 ug/1
2.0 ug/1
2.0 ug/1
2.0 ug/1
2.0 ug/1
1.0 ug/1
Run# 2 Limits
80-120%
80-120%
80-120%
80-120%
~) ·v-,-v .. ,.,2.
10\ S\c I
J = Indicates an estimated value
8 = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
077
• Accutest Laboratories
Report of Analysis Page I of 1
Client Sample ID: MW-64A
Lab Sample ID: FI0823-2
Matrix: AQ -Ground Water
Method: SW846 8270C SW846 35lOC
Project: GELS, Hendersonville, NC
File ID OF
Run #1 L008963.D 1
Run #2
ABN TCL List
CAS No.
98-95-3
CA.S No,
367-12-4
4165-62-2
118-79-6
4165-60-0
321-60-8
1718-51-0
Compound
Nitrobenzene
Surrogate Recoveries
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
Nitrobenzene-d5
2-Fluorobiphenyl
Terphenyl-dl4
NO = Not detected
RL = Reporting Limit
Analyzed
09/13/01
Result
ND
Run# I
46.%
32%
81 %
72%
69%
87%
E = Indicates value exceeds calibration range
Date Sampled: 09/04/01
Date Received: 09/06/01
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
ME 09/09/0 I OP3816 SL513
RL Units Q
5.0 ug/1
Run# 2 Limits
20-125%
10-125%
35-140%
46-125%
46-125%
49-126%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
014
Accutest Laboratories •
Client Sample ID: MW-64A
Lab Sample ID: F10823-2
Matrix: AQ -Ground Water
Report of Analysis
Date Sampled: 09/04/0 I
Date Received: 09/06/01
Percent Solids: n/a
Page I of I
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units OF Prep Analyzed By Method
Barium 29.7;,B'.T 200 0.94 ug/1 09/13/01 09/19/01 JK SW846 6010B
Beryllium 0 60:B'l./ 5.0 0.22 ug/1 09/13/01 09/19/01 JK SW846 6010B
Lead .1,2,B':y i 5.0 1.2 ug/1 09/13/01 09/19/0 I JK SW846 6010B
Manganese 51 4"S-• ,.,!.. 15 0.26 ug/1 09/13/01 09/19/01 JK SW846 6010B
Nickel 0.80 U 40 0.80 ug/1 09/13/01 09/19/01 JK SW846 6010B
RL = Reporting Limit U = Indicates a result < IDL
ID L = Instrument Detection Limit B = Indicates a result > = IDL but < RL
482
Accutest Laboratories •
Client Sample ID: MW-64A
Lab Sample ID: F 11780-8
Matrix:
Method:
AQ -Ground Water
SW846 8260B
Report of Analysis
Date Sampled:
Date Received:
12/12/01
12/14/01
Percent Solids: n/a
Page I of I
Project: GELS, Hendersonville, NC
Run #1
Run #2
File ID
B0007642.D
DF
1
VOA TCL List
CAS No. Compound
/1--+3-2 Denzene
67-66-3 Chloroform
107-06-2 1,2-Dichloroethane
156,59-2 cis-1,2-Dichloroerhylene
156-60-5 trans-1,2-Dichloroethylene
127-1S-4 T :!~:-:ic~!o:-oet~y!e::e
79-01-6 Trichloroethylene
75-01--i \'inyl c:'.:oriG:.:
CAS No. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
17060-07-0 1,2-Dichloroethane-D4
2037-26-5 Toluene-OS
460-00-4 4-Bromofluorobenzene
ND = Not detected
RL = Reporting Limit
Analyzed By
12/20/01 JG
Result RL
NU 1.0
ND 2.0
ND 2.0
ND 2.0
ND 2,0
41.S 2.0
ND 2.0
ND LO
Prep Date
n/a
Units Q
ug/1
ug/1
ug/1
ug/1
ug/1
,,.,.11 -.:,·.
ug/1
,,,.11 u.::,,'
Prep Batch
n/a
Run# I Run# 2 Limits
98% 80-120%
99% 80-120%
99% 80-120%
106% 80-120%
J = Indicates an estimated value
Analytical Batch
VB329
E = Indicates value exceeds calibration range
B = Indicates analyte found in associated method blJnk
N = Indicates presumptive evidence of a compound
019
Accutest Laboratories • Report of Analysis Page l of l
Client Sample ID: MW-64A
Lab Sample ID: Fl 1780-8
Matrix: AQ -Ground Water
Method: SW846 8270C SW846 35!0C
Project: GELS, Hendersonville, NC
File ID DF
Run #l L0l0083.D l
Run #2
ABN TCL List
CAS No. Compound
98-95-3 Niuubt:nzcnc
CAS /so. Surrogate RecO\ .. eries
367-12-4 2-Fluorophenol
4165-62-2 Phenol-d5
l 18-79-6 2,4,6-Tribromophenol
-I 165-60-0 ~itrnbcnzt:ne-J5
321-60-8 2-Fluorobiphenyl
1718-51-0 Terphenyl-dl4
ND = Not detected
RL = Reporting Limit
Analyzed
12ll8/0l
Result
1'D
Run# l
65%
46~
103%
103%
99%
96%
E = Indicates value exceeds calibration range
Date Sampled: l 2ll 2/0 l
Date Received: 12ll4/0l
Percent Solids: n/a
By Prep Date Prep Batch Analytical Batch
ME 12/17/0l OP4382 SL57l
RL Units Q
j.0 ug,i
Run# 2 Limits
20-125%
10-! 25 o/c
35-140%
~S-125%
46-125%
49-126%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N • = Indicates presumptive evidence of a..<:ompound OJ l
Accutest Laboratories •
Client Sample ID: MW-64A
Lab Sample ID: Fl 1780-8
l\latrix: AQ -Ground Water
Report of Analysis
Date Sampled:
Date Received:
12/12/01
12/14/01
Percent Solids: n/a
Page l of l
Project: GELS, Hendersonville, NC
Metals Analysis
Analyte Result RL IDL Units Df Prep Analyzed By Method Prep Method
Barium 30.2 8' -s 2 200 0.94 ug/1 12/18/0 I 12/19/01 DM SW846 60!08 SW846 JOlOA
Beryllium 0.22 U 5.0 0.22 ug/1 12/18/0 l 12/19/01 DM SW846 60108 SWS46 3010A
Lead 4.4 B... \J I 5.0 1.2 ug/1 12/18/01 12/19/01 DM SW846 60108 SW846 JOlOA
Manganese 50.4 15 0.26 ug/1 12/18/01 12/19/01 DM SW846 60108 SW846 JOlOA
~ickd 0.80 G iv 0.80 ug;l 12/ l8,0l ll1 !910! DM SW8-l6 oUluB SW846 30lOA
0032
RL = Reporting Limit U = Indicates a result < IDL
ID L = lnstrument Detection Limit B = Indicates a result > = IDL but < RL
042