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HomeMy WebLinkAboutNCD062555792_20000331_Sigmons Septic Tank Service_FRBCERCLA PA SI_Expanded Site Inspection Report Volume II References 1 - 24-OCR', I I I I I I I J I ~ I I I = = I I I ·I I •• I 0 ' ' . c:-,... =: D-c, - STATE OF NORTH CAROLINA Depa,tment of Environment and Natural Resources Division of Waste Management Superfund Section EXPANDED SITE INSPECTION VOLUMEll-REFERENCES Sigmon's Septic Tank Service NCD 062 555 792 Statesville, Iredell County, North Carolina Reference No. 0406611 l\farch 2000 Stephanie K. Grubbs Hydrogeologist Il Division of Waste l\fanagement Superfund Section I I I I I I I I I I I I I I I I I I I REFERENCES I. United States Environmental Protection Agency. 40 CFR Part 300, Hazard Ranking System:.Final Rule, December 14, 1990 2. United States Environmental Protection Agency, Superfund Chemical Data Matrix 3. 7.5 Minute USGS Topographic Quadrangle Maps of Troutman (1993), Catawba (1970), Statesville (1993) and Stony Point (1970), North Carolina. 4. Grubbs, Stephanie K., NC Superfund Section, Latitude and Longitude Calculation Worksheets, Sigmon's Septic Tank Service Site, March 22, 2000. 5. Grubbs, Stephanie K., NC Superfund Section, Memorandum to File: On site Reconnaissance of the Sigmon's Septic Tank Service Site, November 11, 1999. 6. Wilson, Donna, NC Superfund Section, Memorandum to File: Telephone Conversation- Iredell County Tax Assessor's Office. September I, 1998. 7. Wilson, Donna, NC Superfund Section, Memorandum to File: On-site Reconnaissance, Sigmon's Septic Tank Service. January 20, 1998. 8. Moore, Douglas, NC Superfund Section, Removal Evaluation and On-Site Reconnaissance. Sigmon's Septic Tank Service. December 17, 1996. 9. Grayson, Susan, Departinent of Human Services, Minutes of Meeting in Statesville, NC. June 20, 1980. 10. North Carolina Department of Natural Resources and Community Development. Drilling Well Record. September 8, 1980. Analytical sampling results, September 12, 1980. 11. Sigmon, Henry. Environmental Protection Agency Hazardous waste Notification Form, Part A, November I 0, 1980. 12. Sigmon, Mary. Section 3007 RCRA Questionnaire for United States Environmental Protection Agency. June 11, 1981. Zeller, Howard (US EPA). Letter to AAA Enterprises, Inc., Mary Sigmon, Regarding Section 3007, Resource Conservation and Recovery Act (RCRA) Request for Information. June 5, 1981. 13. Sigmon, Mary, AAA Enterprises, Letter to Bill Meyer Regarding Deletion as a Transporter and Generator. April 19, 1982. I I I I I I I I I I I I I I I I I 14. North Carolina Department of Natural Resources and Community Development, Division of Environmental Management. Monitoring well sampling results. September 24, 1987. June 14, 1990. May 5, 1993. Bold Research Labs. Monitoring well sampling results February 21, I 99 I. 15. North Carolina Department of Natural Resources and Community Development, Division of Environmental Management. Monitoring well construction record. August 31, 1987. 16. North Carolina Department of Natural Resources and Community Development, Division of Environmental Management. Sample Analysis of Lagoon Sample. March 4, 1987. 17. Reading, Scott, Waste Management Specialist, North Carolina Hazardous Waste Compliance Unit. Memo to Keith Masters, Western Area Supervisor, North Carolina Hazardous waste Compliance Unit, Regarding Site Investigation of AAA Enterprises. September 14, 1990. 18. North Carolina Department of Natural Resources and Community Development, Division of Environmental Management. Sample Analysis and Health Risk Evaluation for the Cascadden well. January 27, 1991, November 13, 1991, September I, 1992, February 22, 1993, March 6, 1995, and April 8, I 997. I 9. North Carolina Division of Environmental Management. Sampling Analysis and Health Risk Evaluation for the Davidson well. September I, 1992, October I 0, 1995, and April 7, 1997. 20. North Carolina Division of Environmental Management. Sampling Analysis and Health Risk Evaluation for the Sheppard (current owner) well. February 22, 1993, March 15, 1994, March 6, 1995, October 10, 1995, October 7, 1996, and April 8, 1997. 21. Glasner, Bob, Pete Doorn, Gray Stephens, Laurie Martin, Lafayette Atkinson, North Carolina Hazardous Waste Section. Field Notes and Sampling Analysis. August 31 and September I, 1992. 22. Holyfiled, Doug, Head, Waste Management Branch, North Carolina Division of Solid Waste Management. Memo to Dexter Matthews, Chief, Solid Waste Section, regarding the referral of the AAA Enterprises Site. February 11, 1993. 23. Department of Environment, Health, and Natural Resources, Division of Environmental Management. Monitoring Well Sampling Analysis. June 30, 1993. 24. Smith, Brenda, Regional Supervisor, North Carolina Division of Environmental Management. Letter to Barry Sigmon Regarding Notice of Violation. July 13, 1993. 25. Burrows, Steven M., Project Manager, Shield Environmental Associates, Inc., Sigmon Septic Pit Lagoon Sludge Sampling Report. November 3, 1993. I I I I I I I I I I I I I I I I I I I 26. Cornell, Karen, Hydrogeologist, North Carolina Division of Environmental Management. Memo to Pat DeRosa, North Carolina Superfund Section, Regarding Waste Pile Referrnl. December 15, 1995. 27. Homsley, T.C., Jr., Attorney, Homsley, Jones, Gaines & Fields. Letter to Keith Overcash, Regional Supervisor, North Carolina Division of Environmental Management, Regarding Termination of AAA Enterprises. February 19, 1996. 28. North Carolina Solid Waste Management Section, Septage Management Program. Application for Permit to Operate a Septage Management Firm. May 12, 1984. 29. DeRosa, Pat, Head, Site Assessment and Removal Branch, North Carolina Superfund Section. Letter to Cindy Gurley, Project Officer, U.S. EPA Region IV, Regarding CERCLIS Addition. December 12, 1996. 30. Lair, Myron, Chief, Emergency Response and Removal Branch, U.S. EPA Region IV. Letter to Jack Butler, North Carolina Superfund Section, Regarding Removal Eligibility. April I, 1997. 31. Combined Preliminary Assessment and Site Inspection, North Carolina Superfund Section, Sigmon's Septic Tank Service. September 1998. 32. Grubbs, Stephanie, North Carolina Superfund Section, Memo to File Regarding the 1999 Expanded Site Inspection Sampling Event. December 20, 1999. 33. North Carolina Department of Conservation and Development. Geology and Ground Water in the Statesville Area, North Carolina. Groundwater Bulletin 68. Prepared by Harry E. LeGrand, Geologist, U.S. Geological Survey. 1954. 34. United States Department of Commerce, The Climatic Atlas of the United States, 1983. 35. Grubbs, Stephanie, North Carolina Superfund Section. Memo to File: Water Supply Lines. March 16, 2000. 36. Grubbs, Stephanie K., North Carolina Superfund Section. Memo to File: Public Water Supply data of Community wells within the 4-mile radius of the site. Sigmon's Septic Tank Service. March 3, 2000. 37. Grubbs, Stephanie, North Carolina Superfund Section. Memo to File: Number of People Drinking Water within a 4 Mile Radius, Sigmon's Septic Tank Service. March 23, 2000. 38. North Carolina Administrative Code, Department of Environment, Health, and Natural Resources, Division of Environmental Management, Title 15A Subchapter 2L, Classifications and Water Quality Standards Applicable to the Groundwaters of North Carolina. November 8, 1993. I I I I I I I I I I I I I I I I I 39. United States Federal Emergency Management Agency. Flood Insurance Rate Map, Iredell County, North Carolina, Community-Panel Number 370313 01 SOB, Panel 150 of 220. May 15, 1980. 40. Wilson, Donna, Superfund Section, Memo to File: Flow Rates 15-Mile Surface Water Pathway. Sigmon's Septic Tank Service. March 24, 1998. 41. Grubbs, Stephanie, North Carolina Superfund Section. Memo to File: Fishery Identification along the 15-mile Surface Water Pathway. Sigmon's Septic Tank Service. March 23, 2000. 42. Wilson, Donna, NC Superfund Section, Memo to File: Stream Classifications. Sigmon's Septic Tank Service. June 10, 1997. Classification and Water Quality Standards Assigned to the Waters of the Catawba River Basin, Division of Environmental Management, February 1, 1993. 43. Grubbs, Stephanie, NC Superfund. Memo to File: Davidson Pond. Sigmon's Septic Tank Service. December 20, 1999. 44. U.S. Department of the Interior, Fish and Wildlife Service. 1995. Wetland Inventory Maps. Catawba and Troutman Quadrangles. 45. Grubbs, Stephanie, NC Superfund Section, Memo to File: Threatened and Endangered Species. Sigmon's Septic Tank Service. March 23, 2000. 46. Grubbs, Stephanie, NC Superfund Section, Memo to File: Number of Workers on the Sigmon's Property. Sigmon's Septic Tank Service. March 23, 2000. 47. North Carolina State Center for Geographic Information and Analysis, Populations and Households. Sigmon's Septic Tank Service. March 15, 2000. 48. NC Department of Environment and Natural Resources, Division of Waste Management, Superfund Section, Inactive Hazardous Sites Program, Guidelines for Assessment and Cleanup pursuant to the Inactive Hazardous Sites Response Act of 1987 (N.C.G.S 130A-3 l 0 et.seq.), July 1997. 49. DeRoller, Chris, Division of Environmental Management, Letter to Mr. Barry Sigmon, AAA Enterprises, Regarding the Groundwater Sampling Results. Sigmon's Septic Tank Service. April 8, 1991. 50. Sigmon, Barry, AAA Enterprises, Letter to Karen Walker, Division of Environmental Management, Regarding Lagoon Closure Activities. Sigmon's Septic Tank Service. April 26, 1995. 51. Stanley, Jeannette, NC Superfund Section, Memo to Superfund Section Staff: Update on the Status of the Wellhead Protection Program in NC. April 23, 1999. I I I I I I I I I REFERENCE 1 I I :I I I I I I I I I f6ut Jct1s f/A-f/12-f ·ftc11~"!) -·;-:"_-;:..=.=--·--. -----.. --- Ref. 1 Friday December 14, 1990 Part II Environmental Protection Agency 40 CFR Part 300 Hazard Ranking. System; Final Rule I I I I I I I I I REFERENCE 2 I I I I I I ' I I I I I .. I . I I I I I I I I I I I I I I I Ref. 2 SUPERFUND CHEMICAL DATA MATRIX APPENDIX B TABLES 'age 8-1 >CDM Data VersiOn: JUf.196· i9 AUG 96 HAZARD RANKHIG SYSTEM Hai:ardous Substance Factor Values 376 Substances Ground ',Jater Hobi Li ty \ B ioaccun.ilat ion Liquid Non liquid Persistence Food Chain Envi rormenta l Ecotoxicity Substance Name \cenaphthene :.cenaphthytene Acetaldehydc Acetone -'lcetonitrile -'lcetophenone \cetyl-2-thiourea,, 1- ,,,'' ~crolein -'lcrylamide ;crylic acid -'lcryloni tr\ le i 1: f· Adipic acid (l, .. ;, ,, CAS Nurber Toxicity Karst Non-Karst Karst Non-Karst River Lak:e Fresh 000083-32-9 000208-96-8 000075-07-0 000075-05-8 000098-86-2 000591-08-2 1000 10 100 10 10 000107-02-8 10000 000079-06-1 10000 000079-10-7 10000 000107-13-1 000124-04-9 1000 1.0E+00 1.0E+00 1.0E+00 1.0E+00 1.0E-02 2.0E-01 2.0E-03 0.4000 0.4000* 500.0 .0E+00• 2.0E-01 2.0E-01• 0.4000" 1.0000 .0E+00 1.0E+00 1.0E+00 0.4000 0.0700 1.0E+00 1.0E+00 1.0E+00 0.4000'* 0.0700 1 .0E+00 1.0E+00 1.0E+00 1.0E+00 1.0E+00 1.0E+00 1.0E+00 0.4000* 0.0700 1.0E+00 1.0E+00 1.0000 1.0000 1 .0000 1.0000 1.0E+00 1.0E+00 1 .0E+00 0E+00 0.0700 0.0700 1.0E+00 1.0E+00 .0E+00 1.0E+00 1.0000 1.0000 1.0E+00 1.0E+00 .0E+00 1.0E+00 1.0000 0.4000* 1 .0E+00 I .0E+00 1.0E+0Q 1.0E+00 0.4000 0.0700 1.0E+00 1 .0E+00 1.0E+00 1.0E+00 1.0000., 0.4000., .1.0E+00 1.0E+00 1.0E+00 1.0E+00 1.0000* 1.0000* 500.0 0.5 0.5 0.5 5 .0 0.5 500.0 5.0 0.5 50.0 0.5 5.0 Salt 500.0 500.0 0.5 0.5 0.5 5 .0 0.5 500.0 5.0 0.5 50.0 0.5 5.0 Fresh 500.0 500.0 0.5 0.5 0. 5 5 .0 0.5 500.0 5 .0 0.5 so.a 0.5 5.0 Hdicarb Aldrin 000116-06-3 000309-00-2 000107-18-6 000107-05-1 1000 10000 100 10000 1.0E+00 1.0E+00 1.0E+00 1.0E-04 1.0E+O0 1.0E+00 2.0E-03 2.0E-07 1.0E+00 1.0E+00 1.0E+00 1.0E+00 1.0000 1.0000 50000.0* 50000.0 .. 50000.0 -'lllyl alcohol .\lunim.m ~lU11inun Ar.moni a 007429·90-S 020859-73-8 007664-41-7 10000 1.0E+00 1.0E+00 .0E-04* 1.0000 0.4000 0.4000 0.4000 1.0000 1.0000 1.0000 1.0000 1.0E+00 1.0E+00 l .0E+00 1 .0E+00 0.0007 0.0700 Indicates diffo;'.'ence between previous version of chemical data ( JU"194 ) and current version of chemical data ( JU"196 ). Indicates neiJ hazardous substance in current version of chemical data ( JWl96 ). - ' . i\ I, I -- - - -- -- - 0.5 5 ,0 so.a 0.5 0.5 0.5 5 .0 50.0 0.5 0.5 0.5 5.0 50.0 0.5 0.5 - Salt Fresh ·Salt 500.0 500.0 0.5 0.5 0. 5 5 .0 0.5 10000 10 100 500.0 10000 5.0 0.5 50.0 0.5 5 .0 50000.D 0.5 5.0 I/ so.a 0.5 0.5 100 10 10000 10000 1000 1000 100* 100* 100 10 1000 10 100* 10 10000 10000 1000 1000 100* 100* Air Gas Air Gas Migration Mobility Gas Part 11 11 17 17 17 11 17 6 11 17 0 11 17 NA 17 0.2000 Yes Yes 0.0200 Yes Yl!s 1.0000 Yes No 1.0000 Yes "10 1.0000 Yes Ho 1.0000 Yes No NA No Yes 1.0000 Yes Ho 0.2000 Yes Yes 1.0000 Yes Ho 1.0000 Yes Ho 0.2000* Yes Yes 0.0200 Yes Yes 0.0020* Yes Yes 1.0000 Yes Ho 1.0000 Yes Ho NA No Yes No Yes 1 .0000 Yes No - ---- I I I I I I I I I I REFERENCE 3 I I I I I •• I I I I I I I I I I I I I I I I I. 1· I I I I I Ref. 3 7.5 USGS Quad maps of Troutman (1993), Stony Point (1970), Catawba (1970), and Statesville West (1993), North Carolina. I I I I I I I I I I REFERENCE 4 I I I I I I I I I Ref. 4 1-. ff•.• ,(',C'; CC C :fcff \';;,,';i~i{f &f'~~i:f,',';;',.'::',~"EiJ{if Ei;{,;'. ;',C ;/\ " ?iJ~i; I I I I I I I I I I I I I s·9m0Yl 1) Se¢70 TuttL '.S<YV1ct, CERCLIS I: N© t'Jo1'557> rfcL · SSID: SITE NAH.E: AXA: -------------- ADDRESS, Ld.&8 WfQI 0--{2.._J. . CITY: S/-rJJJ1lV/ I Le. . STATE; NG ZIP CODE: ~r'A~_1_7_{.p~---- SITE REFERENCE POINT, /IJE-Corr1.e,c 4i la~, /U'flG uses QUAD KAP NAHE: TY1Jl!~ TOWNSHIP: __ N/ s RANGE, E/W ·-------------------------- SCALE:_ 1: 24, o_oo KAP. D~~~; - - - iq13 SECTION: 1927 a(CIR.CLE· ONE) fl.AP DATUH: HERIDIAN :· -----------~------ COORDINATES .FR.OK LOWER RIGHT (.SOUTHEAST) CORNER OF 7. 5' KAP (attach photocopy): LONGITUDE: ~o ~-3Q__• LATITUDE: ,32..._0 31 ' 3Q__" COORDINATES FR.OH LOWER RIGHT (SOUTHEAST) CORNER OF 2.5' GoID CELL: LONGITUDE: /!JQ_o .:51_•· CJf:i_" LATITUDE: fil__o 4--2 ' 3D_" CALCULATIONS: LATITUDE (7.5' QUADRANGLE KAP) A) NUHBER OF RULER GRADUATIONS FROH LAT!TUDS GRID LINE TO SITS REF PG.,NT: q1e_ S) HULTIPLY (A) BY 0.3304 TO CONVERT TO SECONDS: AX 0.3304 C) EXPRESS IN HINUTES AND SECONDS ( l '= 60"): J)Q_' 3;2_.. _If.a_•· D) ADD TO STARTING LATITUDE: 2f5 ° 4d..' a) , OU " + 00 •~-Du_ SITE LATITUDE: 35:__o_!fi• _il._f2Q_" CALCULATIONS: LONGITUDE ( 7. 5' · QUADRANGLE /-'.AP) _A) NUHBER OF RULER GRADUATIONS FR.OH.RIGHT LONGITUDE LINE TO SITE REF POINT: B) HULTIPLY (A) DY 0.3304 TO CONVERT TO SECONDS: AxO.JJOt1 & ~f:. . I ' 'I I I I r I ' I " I , ' ~ I . I C I i I I I I I I I I \I REFERENCE 5 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I MEMORANDUM DATE: TO: FROM: RE: November 11, 1999 File Stephanie K. Grubbs 1.-h - 1-lydrogeologist ,l?JO,.f/rttUW NC Superfund Section On-site Reconnaissance Sigmon's Septic Tank Service NCO# 062 555 792 Ref. 5 On November 11, 1999 al 11 :00 am , Harry Zinn and I arrived at Sigmon's Septic Tank Service in Statesville, NC. We met with Mary Sigmon, the current owner of Environmental Services Inc. She stated that her mother is the owner of the property where the lagoons arc located but she is the current owner of the business. Harry and I gave her a copy of the text portion of the Combined PA/SI and informed her that if she would like to view the entire file she should make a FIOA request with Scott Ross. She then gave us permission to investigate the property including the trench and waste pile areas. We then walked along the trenches and determine the locations for sampling. The trench areas were obvious with stressed vegetation and waste products visible on the surface of the lagoons. We located all the trenches 1-8 based on Donna Wilson's pictorial in the PA/SI. At noon, we drove around to Mustang Drive, east of the site to the trailers at the end of the road. Mr. George Lees is the current owner, Mr. Frye was the previous owner during the PA/SI. Mr. Lees address is 130 Mustang Dive, Statesville, NC 28677. He gave us permission to sample his well. He stated that there is a filter at the well head for trapping sediment and that it could be by-passed for sampling. He also stated that the owner of the property, Steve Lambreth, was going lo install a new well for additional mobile homes south of the properly, even closer to the Sigmon's trenches. He stated that every two mobile homes share a common well. After we left Mustang Drive, Harry and I drove to Lauren Drive, the dirt road south of the Sigmon property. We drove past the Davidson pond and did not observe any indication of fishing. We proceeded to drive to the mobile homes along Lauren Drive that have contaminated drinking water wells. We drove to the end of Lauren Drive and left a card for the owner to contact us if they wanted to have their well sampled. This property was quite far from the Sigmon's property but still within a target range. I I I I I I I I I I I I I I I I I I We then drove down Lauren Lane and stopped at 173 Lauren Drive. The mobile home was not occupied and we also left a card with a name and number to be contacted. Across from that property is a sign that states that the Sigmon's property is a septage waste disposal area and do not trespass. As we drove down Lauren Drive, we passed the Davidson pond and inspected the drainage ditches from east and west of the pond. The east side of the ditch drains the Davidson property and will be sampled for attribution. The Davidson Roofing Company phone number is (704) 528-6 I 92. Harry and I left the site at I :00 pm for Raleigh. 11\1h1 - 1)}\ y\/ (11,\ -~b ,{A I tu .. •~. I -1.i:I ·,:L I \...,_,. -------- Ir, .. ~R/SI , (011')_ _-kfC _,0-i~• -----. . ~ . ',', j_1 c{Q:(UH (I~ !__tth. ir t~V1\cL l. J~)i,(~ ...Q.lf'/i.".~- -,, ' ' -· ' I ·-----··-----·••-------------.. --~--/ ---·-1 .. --· -·-· .. 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I ~t!J'. 0 -I;-, •l~. ].U '>Oh C ,., ~ = - .. _. <-s ~ loo ,;f< c\ s-tic { J'i,Ju..1_1J-"' J3o \'"<" J,!v . L rA s;, i ';(; ("" ~:,_ J . ·:,to:· -: -b,; ,L ( ,, I I 6 ·,,_ u1::;<.:.. /,\_ w -◊r-, ,( I'-. -~ _:l_lfj, R,:,'-.'a:';C c=;_ :62.__Q, ~t ,....-,-,Jy{< ~ >. ). ~~ -2> I I I I - ------------ I I I I I I I I I I I REFERENCE 6 I I I I I' I I I I znr To: From: Subject: Date: MEMORANDUM File Donna Wilson 'py,t ,~5r-{ {~5t,- Environmental Engineer '· North Carolina Superfund Section Ref. 6 Telephone conversation -Iredell County Tax Assessor's Office Sigmon Septic Tank Service Statesville, Iredell County September 1, 1998 On December I 0, 1996, Doug Moore of the North Carolina Superfund Section spoke with Linda cifthe Tax Assessor's Office (phone 704-878-3012) regarding the Sigmon property. The property consists of 15.35 acres and is owned by Mr. Henry Sigmon of 1268 Eufola Road. The parcel is listed as A24 on tax map 3Q. Mr. Sigmon purchased the property in 1970 from Robert C. Hammonds (Book 491, page 389). The property may have been split to Mary Sigmon in 1996; however, the split had not been recorded on the deed at that time. A copy of the tax map is attached. I I I I I I I I I REFERENCE 7 I I I I I I I I I I I To: From: Subject: Date: MEMORANDUM File Donna Wilson ~v Environmental Engineer )\, North Carolina Superfund Section On-site reconnaissance Sigmon's Septic Tank Service Statesville, Iredell County January 20, 1998 Ref. 7 On August 14, 1997, Stuart Parker and I traveled to the above referenced site to conduct an on-site reconnaissance. We arrived at approximately 3:00 and met with Paul Dahlen of the Mooresville Regional Office, Groundwater Division. Mr. Dahlen informed us that a mobile home development (consisting of 6 homes) had recently been constructed adjacent to the Sigmon site. His office had not yet sampled any of the wells in the development. On the east side of the Sigmon property there is a opening in the fencing by one of the new trailers. We talked with the resident of the first trailer east of the Sigmon site, Merle Potts, whose address is 1280 Eufola Road. All of the trailers in the new development, including his, have individual private groundwater wells. The former resident of this trailer was Robertson. The Davidson Roofing well was last sampled by the MRO in April. The Davidson home, address 2057 Buffalo Shoals Road, is just north of the Davidson Roofing business. Chris Davidson owns and leases out the four homes west of his business on Lauren Drive. Davidson alleged that an earlier tenant of his, Ellmore, dumped a gas tank on the property (132 Lauren Drive), resulting in semi-volatiles getting into the water lines. Soil was removed and subsequent testing was conducted. As a result of this problem, Chris Davidson installed 2 monitoring wells at 172 Lauren Drive, across the street from 132 Lauren Drive, and a new domestic well, now located by his business. He gave us permission to sample any of his wells. Memo to File Sigmon's Septic Tank Service January 20, 1998 Page 2 ·---------------·. --- We stopped and spoke with the resident of 183 Lauren Drive, Tom Shepperd, and received permission to sample the well. Phyllis Frye died since the last sampling of the well. At 3:50, we met with Mary Sigmon. Ms. Sigmon does not know the details of her well, and the top is covered over with concrete. The water from the well is not treated or filtered. She stated that there are 5 workers onsite. The sludges are no longer being landfarmed. They currently take waste from residential pumpers and three grease traps. She doesn't know the contents of the drums that are in and near the shed on the eastern edge ofthc property. The septic field for the house is directed to the east, and the septic line for the office trailer is directed to the south. She has no knowledge or information concerning the two small open pits that are located in the extreme southeast corner of the site. East of the office, near the entrance road, is a square metal basin, buried in the ground, except for the top edge. Mary Sigmon stated that the basin is used to solidify certain pumpmgs. At 4:20, we drove to an area past the office, north of the shed, that contained drums. Photos 8 . IO were taken in this area. The drums are stored cast of the driveway and there is a soil stain on the road nearby that is approximately 3 feet by 6 feet. Eight drums were noted, and are described below: Shellzonc antifreeze• 55 gallons full, dated 8/18/89 Elgene's Fabulene • approx. 1/4 full. Mamaroneck, NY I 0543. Tank dipping, cleaner. Gray plastic drum• "SON" painted on side, ½ full. Chevron Delo 400 l 5W40 motor oil, possibly empty Hydrotex Dallas Tex lubricant· empty Rusted drum, oily white, punctured. Full 2 drums, rusted, full, contents unknown At 4:42 we investigated drums in a shed. Photos 11-13 were taken. There were approximately 20 drums, positioned upright and lateral. At least half of the drums were full, all were sealed, and none were marked. The drums were covered with straw and debris. Four above ground storage tanks are near the shed and are used for the storage of septic pumpings. According to Mary Sigmon, when the tanks are full, the contents are pumped f'· .. -.' , .. , :~: i ~ ,. 11 ,. 11 11 ti 11 ;,1 :I I I I I I l I Memo to File Sigmon's Septic Tank Service January 20, 1998 Page 3 and transported to a wastewater treatment facility. Photos 14-15 were taken of the tanks. The tanks are positioned laterally, diameter 10. feet, and approximately 20 to 25 feet long. The po11s are at the top edge. The bottom of the drums are buried approximately 2 feet. At 5:00, we drove to the Frances Lamberth residence at 152 Lamberth Ridge Drive (phone 704-528-4623), which is located just west of the Sigmon Property. She gave permission to sample her well and said that her well was sampled about 5 years ago. The well is approximately 56 to 62 feet deep. Mrs. Lamberth stated that the well is on an "underground river" which flows to the small pond to the north, not the pond to the west. The pond to the west, the Williams pond, is downstream. She said that the first house on Lamberth Ridge Drive was owned by Mike Lamberth and the second house was owned by Wade Lamberth. Both of those houses utilize one well which is located under Wade Lamberth's house. She said that the log cabin that is currently being built on Eufola Road near the site is owned by Richard Teague. From 5:30 to 6:00 we conducted a house count along Eufola and Buffalo Shoals Roads. The total number of offsite houses within 1/4 mile was 35. At 6:00, we stopped by 117 Green Valley Road and obtained permission from the owner of the house to walk across the property to sample Norwood Creek. At 6:25, we stopped by 2192 or 2194 Buffalo Shoals Road to get permission to sample the background pond. No one was home. Two mailboxes were near the driveway, apparently including the resident across the street. "Broom" is printed on-one of the mailboxes. We left the site at 6:30. ,- 1 I I I Q g or fm~ ce, laMb01.-fl._ D ~11 lo I '~w 1 a o 1 11 a I] Q /4 lvulL 't) ';::(L,.J u ,_ -,,., I lliJ. C /'jU TT, /:,?. [J I 2-4 0 CJ 'f5> =-.: • l """',t-L"JC----Ci --- L .,.--:. -------i-~--J----t-r--:c-:----:-;f-----::-c-:-c':-:-ih"'----'\.--:1,-:c·.1" ·. ~ 1~,-----t---=---t----j-..:.._--1-----f---- (~. ---J---.1'f.-:'-~~--jr'7-~-;:-J-L----,-;-:-t~-:-, -' . I;. onJ, '.:--1\•~":-'--""Lf:.~1-------,-;;--J--c---'--+--,.;:----~~-,-f'i !----: ~ ...,,J',. ~ ;_,.., ---,---j I I fty- I I I I I I I I I REFERENCE 8 I I I I I I I I I I T 77 Memo Date: December 17, 1996 To: From: File Douglas Moore Environmental Chemist NC Superfund Section ZO?MC:CO emmsw Re: Removal Evaluation and On-Site Reconnaissance Sigmon's Septic Tank Service 1268 Eufola Road Statesville, Iredell County, NC US EPA ID: NCD 062 555 792 Ref. 8 On Monday, November 16, 1996, Rusty Harris-Bishop and Douglas Moore of the NC Superfund Section traveled to the subject site to conduct an on-site reconnaissance. We departed Raleigh at 08:45 and arrived at the site at 11 :45. Upon arrival, we met with Mr. Paul Dahlen, Groundwater Section-Mooresville Regional Office, Mr. Henry Sigmon, Jr., site owner and former operator, Ruby Sigmon, Mary Sigmon, owner of Sigmon Environmental Services and current site operator, Mike Gill, office manager of the Sigmon Environmental Services. Doug Moore discussed the purpose of our visit to conduct a preliminary onsite reconnaissance for a removal evaluation. Mr. Henry Sigmon discussed the site history. Sigmon's Septic Tank Service (Sigmon's) has been in business since 1948. Henry Sigmon purchased the property and moved the operation to the site around 1970. Sigmon's business consisted on pumping septage wastes from mostly residential septic tanks, plus some industrial septage from area businesses. Specifically, Mr. Sigmon mentioned that they took septage from Zimmer Industries (a medical supplies company) and Ro-Mac Company (a metal treating business located in Troutman, NC). Sigmon's was a wholly-owned subsidiary of A.A.A. Enterprises. Between 1970-1978, Sigmons emptied wastewaters to the City of Statesville sewer. Around 1973-74, Sigmon's received permits and land applied sludges to area fannlands. Mr. Sigmon stated that the materials they land applied were essentially the same as the materials later placed in lagoons at the site. Around 1978, Sigmons dug several lagoons at the site and began placing septage wastes inside these lagoons. Mr. Sigmon stated that he had received verbal permission from Rawlin Johnson of the Iredell County Health Department and from representatives in the Mooresville Regional Office to construct and use the lagoons for septage disposal. No permits were issued for the lagoons. It is Mr. I I I I I Sigmoo's ooo<~,: he is""' ~spoosib<e foe~, eo,=;,.;,., Soee <hese lagooos were verbally approved by the Iredell County Health Department. The lagoons were actively used until around I 992. Mary Sigmon stated that Sigmon's filed Chapter 11 reorganization in the l 980's and operated until 1995, when the company was forced to cease operations by the Internal Revenue Service for "financial reasons". At that time, Mary purchased two trucks from Sigmon Septic Tank Service and started her own business as "Sigmon Environmental Services, Inc." in January 1996. Both Sigmon's Septic Tank Service and it's parent company, AAA Enterprises, are no longer operating businesses. Following the discovery of groundwater contamination at the site, Sigmons provided bottled water to the affected residents until the early I 990's. Mr. Sigmon stated that Florence Russell had a mean dog and that instead of Sigmons transporting the water to the homes, he left the bottled water on the porch of his own residence at 1268 Eufola Road for the residents to pick up on their own. He stated that the residents stopped picking up the bottled water and so he therefore stopped supplying the water. Mr. Paul Dahlen slated that he spoke with Mrs. Rachel Brown that morning, the current resident of the former Russell residence, and that Mrs. Brown is purchasing her own bottled water. Paul Dahlen stated that he had the Iredell County Sheriffs Dept. serve papers to Mr. Sigmon's son, Barry Sigmon, requesting that Sigmons re-supply bottled water to the affected residents again. He stated that he has been unsuccessful in serving the papers at this time. Mr. Sigmon's contention is that he is not responsible for the groundwater contamination at the site. At 12:40, we drove to the former lagoon area. The lagoons were sited on the crest of a east to west trending ridge that appears to be a high point for the general area. Surface runoff from the site could flow radially in several directions from northwest to east-southeast, although the primary overland runoff from the site appears to travel northwest. In 1993, Shields Environmental (Shields) of Winston-Salem was contracted by Sigmon's to address the environmental concerns associated with the site. At that time, Shields had Sigmon's remove the sludge from the lagoons, mix it with sawdust and stockpile the sludge on a plastic sheet near the southeast comer of the site. There are no surface caps or covers on top of the waste pile. A second pit was dug in an open pasture to the north of the former lagoons which Shield intended to line with plastic as a temporary holding pit while they aerate the sludge. Although the pit was constructed, the remedial phase of the project was never started, primarily due to differences between Mr. Sigmon and the project managers of Shields. Mr. Sigmon stated that they excavated all the sludges from the lagoons to a depth of 10 feet and then backfilled the lagoons with clay fill from the small pond located north of the main office. Mr. Sigmon did not know whether Shield collected post-removal soil samples from the base of the excavated lagoons. Henry Sigmon stated that during the excavation, they encountered large boulders and sandy soil within 2 feet of the base of the lagoons. The presence of bedrock could not be confirmed at this location, but is suggested by the boulders. 2 I Doug Moore measured the approximate dimensions of the former lagoon area. Based on the evidence of backfill, the dimension were measured with a large hand wheel. The areal dimensions are approximately 213 feet long, by 247.5 feet wide, or 52,717.5 square feet (1.21 acres). The lagoon area is covered with grass and vegetation. The lagoons are surrounded by a three strand barbed wire fence and posted with signs that read "Keep Out. Sewage Disposal Area". However, it was evident that people had been trespassing onto the former lagoon property at the southwest corner and Lauren Drive. A large hole had been cut in the barbed wire fence and tire tracks were visible entering the property through the hole. Mr. Gill stated that they have problems with people trespassing onto the property with either four-wheel drive vehicles or All-Terrain Vehicles from Lauren Drive. At 13:30, Doug Moore, Paul Dahlen and Rusty Harris-Bishop inspected the two downgradient wells at the Mike James and Rachel Brown residences. These two residences are rental properties. The Rachel Brown well is a bored well, roughly 30 inches in diameter. A jet pump and reservoir tank connected to two PVC drops pipes are installed at the wellhead: The depth to groundwater was visually estimated to be approximately 27 feet in the bored well. Mr. James was not home at the time of the inspection. We opened the wellhouse to observe the well construction. There were no tags visible at the wellhead. The well appears to be a 6 inch drilled well with a jet pump and reservoir tank installed at the wellhead. No additional information could be obtained at this time. The two wells are approximately 400 feet southwest of the site. At 13 :50, Doug Moore measured the dimensions of the wastepile by pacing the circumference at the base of the pile with the hand wheel. The circumference was approximately 346.5 feet and-the pile was approximately 15 feet tall. One estimate was that the pile contained approximately 2000 tons of sludge. I estimated the volume of the wastepile by using formulas for a spherical pile with a height of 15 feet and a radius of 55.147 feet (i.e. circumference/2 x pi). The radius and height were entered into the formula for the volume of a spherical segment: V = 1/6 it•h (3•r2 + h2), or 1/6 7t (15) (3•(55.147)2 + (15)\ By my estimates, the figure would be approximately 2,705 cubic yards (or 2,705 tons). The wastepile has a grass cover. There are several small seeps visible at the base of the wastepile. At 14:05, Doug Moore and Rusty Harris-Bishop walked the overland surface drainage downgradient to the northwest edge of the property. The slopes in this direction have traces of numerous surface seeps and erosion has cut several drainage paths for the seeps. The overland drainage crosses an open pasture to a low drainage feature that directs the runoff to the west-northwest. At the northwest edge of the property, a small earthen berm (roughlyl-2 feet tall) has been constructed to prevent runoff from leaving the site. This area is wet. Deer and cow tracks were observed on the Sigmon property at this location. The surface runoff apparently enters the ground and flows west-northwest where it appears to surface again at the Lamberth property immediately west of the site. The 3 runoff is then directed to the northwest towards a small pond located on the Wade Lamberth property. At 14: 15, we walked back to the wastepile. Observing the slope of the land from this area, there was no visible evidence of surface runoff to the southeast. However, there are several houses along Lauren Drive southeast of the site. One wellhead was observed in the center of an open pasture behind one of these houses that would be downgradient of the site. This well was formerly used to supply drinking water to the Chris Davidson residence. Historic groundwater samples determined that the well had elevated iron and manganese levels above the State of North Carolina drinking water standards. Since that time, Mr. Davidson has moved to a new house further east and the well was not used for drinking water supply. Mr. Davidson constructed another well at his new location which he uses to supply drinking water for the 4 residences along Lauren Drive, southeast of the site. The current Davidson well was recently sampled by DEM and found to contain trichloroethylene below the State groundwater standards. We also observed a small pond directly opposite the houses on Lauren Drive, approximately 700 feet southeast of the site that could feasible receive groundwater to surface water discharge. This pond most likely contains fish species. The small pond is readily accessible to the residents of Lauren Drive and may be used for recreational fishing. At 14:30, we drove from the site to the office trailer. The former background monitoring well (MW-4) was no longer present along the road bed. Mary Sigmon stated that she is the sole owner of Sigmon's Environmental Service, Inc. and that there are no parent companies. We finished our tour of the site with a brief discussion of the future action with the site. We departed the site at 15:05. At 15:10, we attempted to located the downgradient pond on the Wade Lamberth property. Mrs. Joyce Lamberth granted permission to cross the property and observe the pond. The pond is relatively inaccessible from any nearby roads and Mrs. Lamberth stated that although the pond contains fish species, she has not observed anyone fishing in the pond. We walked to the pond. The pond is located due south from Mrs. Lamberths residence in a low portion of a cow pasture. There was no evidence of any fishing at the pond. This small pond appears to be a watering hole for the Lamberth's livestock. At 15:40, we departed the site for Raleigh. 4 = I■ WWW kLcb:i=i=i=ijjj~j_±±-i-i_-i-i-r_--r_-r_-r_-r_-c_ ~ ----------1--+--1--· -------- .. _.:~-".'.~:.;_-__,..:-_ --_--;--..•.. :, . ..:. ---->· •• • -• • : • C -•• --• ·:mi\};~tl~~litiJr -':))}i~{L: -- . -;••·· . - -----1 I ' I " . ·.:· ~,•;. ( · l •i:.i:: ! 111i;:11 ----~=====~=~=--------- / ·--;r------·/"-•----··-·· _1 __ _ / ·.,\~{(. _i/''' :· ~-h~-+--,-k-+-~~-::4-~~ , ~~'t-+----t--==r--+--'+--"+-+---+---£i\-=J-()./---"J--'+----=~4'l-------+-I~~ f. '----'---'-------'----'-------______L___L__J____J___L____[______j__L____J__J__'.___j__j_______l__l_____L_ ' .. ---------·----. T - I I - I (I --~----J~'i :/ -i -~--- l i\ ~ I ,-N"I --J j I I: ~ v '-'f ' 8--. ~ ..--, ---~ ~ ---. 11 1 1'~ :7 --~---··-· ----· --, \ .c,, ,g .}j\] ___ F_ t ,., \ Uc V',1' '~ ~1 l.{l ---1-: ~: ~ I ----J--J; ---J,I_ -1----1-, -:::r:N1) '-- I i I l ------1~ -::-----'-------- ,.1 t 1~----"-------i-------~--:·i--\ 1 _____________ _] !, _______ _ ·e:·•: ,.,.' . , .• :.-<" . .:rf?rn~tf • - _ -! 1 ('l(f! _1_ --- ,n5 IP·'11c~/~ '1 ~--: ~ ' =--==~= =~--,~~:,~ ,-rYy;ss __ _ ' " ----·----·----------.... '--,,,--cc---- ' ,-.. . -1"'"")'•~-i--, ,, ---- f-1,----j-c,:;1=--1,----tiii::.;J,~c-----;[~ q:,:;pl Vi'JP-. ----·- ··----,--:: "\,> -· -------·-·----------·--··' --'....--~~c------. ..., -----------~'\i,, ------~ ,,~---------,, ' l ;, .j -1 i I ., I \fa--.•~ ... .. ';_\1' j"iq'. l'".L ' . t?~ t,:,.: t~i~1 .. ' ' ! :i~ti,: .. I a llllfDl .. ,.:,:1·,~,;;}\ii1:f!,t,/: :iit::i) ): -------1f . : ~ . ---w...,..o" I ..._r"'-tt-. - J-, -1~•-~ w("W,. I ~'/1=---' 1----l-- ----r:e L+ -~-ff--~=-,=..,+--1----+---a -------f'~-•--.-i .!....._I)( .rd '----'--' ~ i__ik __ ,f-----'--+--"-1------'-=-~ f----+--+-/?-. ---------------------~----- ·---·----------- ·--··-·-·-·-· -~-------··---,--/--~- / _______ [. __ ;,/ / I I I ___ / _____ _ / / .·:,:,,\\);fit. <J· ·.;r I I I I I I I I I I REFERENCE 9 I I I I I I I I I F1277E2 ~ •. ' i ;" ~ .. vr:r smrrv_r ... w ??Xfl/17 _;_;srnr:zr,,,,s??'.?J??1YZ7!?m. Q?i. ,..,9_.,,. M rnsm·· ns / Ref. 9 ~ JAMES B. HUNT. JR. STATE OF NORTH CAROLINA DEPARTMENT OF HUMAN RESOURCES Division of Health Services HUGH H. TILSON, M.D. I GOVl:RNOR S AH T, MORROW, M.D., M,P.H • • l:CRl:TARY I I I I P. 0. Box 2091 Raleigh 27602 Minutes of Meeting in Statesville, NC June 20, 1980 Depth of ponds 10-15 feet (Rollin Johnson) Water table here at 40-50 feet (Steve Steinbeck) Signs of horse dung and hoof prints all over, in beb·1een lagoons. Position is upland, only in one direction is there a rise from this area; in all other directions, the landfalls. Trailer located approximately 400 feet downhill. Whole thing in Sigmon's pastu,e. DIRT ROAD OR DRIVEWAY Approximately 15' to fence 15' x 87' green water 15' X 66 1 green water (obviously some septage addition-tampon casings floating) 75' x 9'. green water DIRl:CTOR ;I I milky white 15' x 200' banked with fill dirt I I I I I I I I IV 1, ,,. I~ ' ; /' ' ; / \.I/ )j', Hillcrest --- 1' 15' 217 feet long milky white, scum on surface. (Water level appears to have fallen one foot) banked at end .1 ;nilky white, hardly any 220 feet long X 211 .cil scum, tampon casings,. banked a w1 e 1 1 eve appears to have dropped tend about a foot Hillcrest 1' tree stump thrown in 1.eve1. appears CO nd.V€ i7' 15' 181 feet long dropped 10-12 II 1 dead banked --!, lots of bubbling weeds protruding at edges .J, Heavy scum layers, level has 133' X 2l'water level has dropped 235' X 21' dropped about about one foot 15-1811 banked all along this side higher than my head,no slope; sheer cliff, n 0 slope,banks were not seeded. Some were growing weeds a .. I i . • -. I ~ ,. ( I ,. "Lii•"&L' Minutes (Statesville· -2-June 20, 1980 Dumping occurred at the site while we were there (11:45 a.m.). Sigmon Septic Tank Service office: 873-8954, home: 528-6321. 90 Diesel Chevrolet, 3800 gallon capacity. Waste smelled industrial, liquid, black. Gentleman driving identified himself as Frank Sigmon, nephew of the man who owns the company. According to Frank Sigmon: They have pumped from Barnhardt, Clark Equipment, Union Glass. Do not use lime for odors -puts out vanilla extract. Have filled in a couple of pits "up the hill". Been using this site for septage since the sewer cut him off and used to put chemicals here. Chemicals would set up solid, doesn't ______________ <:_i~-e~t'=:a:'.:g':e:.:.· _________________ _ cc: Steve Steinbeck Frank Olive Rick Doby/ Susan C. Grayson Project Supervisor ··•'.'· / ' .I I I Ji i I ' I I I i ' i i I I I I I I I I I REFERENCE 10 I I I I I I I I I I I '· I 1: I I I I I I I I I I I I I I .. ,.,,.,.\ (."••-·.n. ... I•'" , DIV] SI o:~ OF ENV I ;:::.01;,v,cNT·AL MMIAGE:•,!:NT, G~ou.•;o· .... ;..TER, SECT I O."I · o,o. COX ?7687 -P.,\1 ... EIGH, N.C. 27&11 (··•. Ref. 10 DR.ILLI:;G· CO?-.""i'RACTOR ( ,J _-, (/ '<"G ·•·o \-,"SLL COfb.1.-RUCTION PER.MIT NO. _,..re.'-"•-·"· 4. TOPOGf'u\PHY: dr.·n,.,vallcy,slopc,hilltopQ0.~Jairclc one) 5. USS or WELL: 7::>¢ DATE:. 9-,:f-J-r.? 6. DOES THIS HELL REPLACE AN EXISTING WELL? __ -'-":/'-~(~) __ _ 7. TOT,\L DEPTH, ,JJ' RIG TYPE OR t-!.£ T 110D :_~/_7'~41+""~•~/_t.._ 8. FQ?.;•\;\TIQ}/ 5;.}\?LES COLLEC7ED: YES NO __ ~•-'----- Depth to ft ~'G?.OUT: Depth Inside Wall thick. type Diu. or weight/ft. ---- Material Method Dia. Type & Oper,ing D'.::PTH FR0->1--TO [J -,y- f-; 3 I ;}·~-::, 3, ,;r;, -:;i. f , JRILLHlG LOG FORHATION o:::sc:nP7ION LOCAT lot~ SKETCH Fro:-:l to ft ____ _ (Sha,._. dist;i:'lc~ to :iu:::bcrcd ro;:lds, or othc:.-~-1p :'e:-'!~c:ic•.: ,io1r:t!;) .J...2_....~cp_;;.;::::L: Depth Size Material 13' 14. F'ro:n ___ to ___ f t ____ _ -. 1-It' nbovc . ST,\TIC W,\T£r\ LEV!-.:L:....:S°:.., f~-1-~rp cf o?¼ ~g --~ ) . -L Casing is ___ ft. ~bovc land surf2ce £LEV: J..5.._ YIELD(gpm) : ______ METHOD OF TESTING: ____ _ )JS. PU:.:?U<G W,\TER LEVEL: ________ ft. :n-:-C:-!LORINATiml: Typc _______ J\mount _____ _ PL':·iP: D«tc Installed _________ _ :-:uke ____________ l ll Luke Deµ th'------ hi r l inc Depth ______ _ l ·-·--·--· _____ j0_r.!/:..1..1 __ ------------- ,c. !i,\S Ti-iL o:·i:lC:R Bf.EN PR.OVItJ[D l\ CO:'Y or TIIIS llf.COKD ,\:,;Q r::?OR,'-lE:D o: T!IE D£P,\RT:-:::::7s H.CQU1R£:-:..:::::;s _;:,.o p_:;co:-:.,1ENDA"i' 1 o:, S? DEPART:·G::1,T OF Ni\TL'RAL A,_\'!) ECO:,mac P..ESOL"'RC::S , ( GROUi\'DlIATER SECTIO~i · 1 ?ie~d -----l'~o~ by: Date 9-.f-:iz) County <-,,h.,,/g c,=a.:::.c.:, "!:own ,S,( c_J~ 2 7i 7 ·p,vy<&-c.:~ .,._,, .:.... Offic ~----uses _____ _ I ,7.e:-&-I~ ,../'r,,___,,..., t../ Driller . {lz;_; dc.L.---t (J D2.te: Drilled 9 -Y---,fV I cl=!' t!, , .., 7 . / ft. ; Diam. I I I( ; . C: l.n.; Cased to ___ ft.; Description c.bovc HSL Thickness (i e:et) I-~---'-/J-'-"l--<-,c=/'--. --'-'/Jl."-'-=~ 7 -.c.=,---:'--C-4---) ( '"'""'. "",,.,'----"'--d;~?Jl---'-"'-t'---'-"'S---=(2.,e~J-'--'. ·_-t=I ~-=· 3---j---'-I 0(-=-· ~--f-, ,---t--'.{u=½.d_f...)_ D-.....,i..<ll<'. ___cJ . i J.. ( _;;;. .r---I ..J "_d / qf I I I . I I . I I I .6. . --It 0 ,_ I I - ;; / ~7' l--7D I •-· c-Jl i--✓' L -d-f';..5 ~ I I I_) I . ------·- I- I I··): 6J. -, -··1 ( ?. ~ ~ :..:: 3 I I I I I I I I I I --==--:-------:--:--::--------:----.,------------------(?=?in g Time, Air Temperature, etc.) ~ Mor ~---------·---------------------------------- Tas:e ---------:------'--------"EST FOR CONSTITUEtiTS OR PROPERTIES AS I:.lECATED. REPORT 0L".LYSIS TO: CHIEF; I .. !.2.'.--..2.lin~ty (As CaC03) -< / I X; to pc! 8. 3 .... ; .... _. ______ ng/ l j )< · to pH 4.5......... rng/1 _.;2.-.=.:!.nu:J..·............. ug/ l -------- .0.:-sse;oic....... .• . . • . . ug/1 -------- ~i=arbo~ate ...... ·•··-~/~f_· ___ ng/1 r __ ,. :::::, 5-Jay ........... ________ ng/1 :v ~ -·-- I '---' !X: Ca:-j~uace ............ ___ ~_/ ____ mg/1 Ca=bo~ Dioxide ........... _______ ng/1 =~~orid~ .•••• ········--~----~g/1 :co~::.fo= (Total lli').. . /lOOc::l --~--- :'.:2.::-0::::;.2s s, ~;:,:: c:2.rbonate..... mg/ l -------- --~··· .. •............. ug/1 --------. _:;..2.:.................. ug/i -------- I : • '.~:::::~~::::::::::: :--------::;: -------- I I~:==~::. r~.ff -v--· I C, •. ~. Nitrogen Kjeldahl .....•••.• _____ ....; c:g/1 Nitrate & ~itrite. D"?,/1 ------' pH \'alue (\s'h2n analyzed {(). Z -~--'--- Phenol ............ : ... . eg/1 ------- i:.g/1 Pot2.ssilliil ............ . ------r::.;;,ll Soecific Cond~~ta~ce • 0 (cicrowhos 2t 25 C) .. ------ Silica .....•..... ; ... -------' ng/1 c:.g /1 Sodi= .....•......•.• ------- 12;;,/ l u--I, C, I .1. Calci= ...••..•... , .. -------' r::.;(i Y.zgr.esiUE ............... . r..3/ 1 ~=-----' R~arks: Toe. I i CJ [2c] D ~ LJ n '---' r-; LJ r-; I I ·--· ~ I ! '----' D I I D n L._I I. I I. I I I I I I I I I I I I I I I I 1. -...-~L:!... LOCA7IC::: (Show stetch of the location belo;.;} ~;e~ rest To•.:n : ___ ~T-f-_,jZcc,: =:i:o:)":.,",-£.::::,c:=,;t. -=.:.__,=-"'----'-/tY='-'-=-----Coun ty: 0 c L ,L/ 7 ~ /7J / 7, ·:; ? Quac:angle No. k-lo ,Z 0-J (Road,Co::-.·:11.: .. ,ity or subdivision and Lot No.) 2. C'o02~1._~,1c_u/c::-J../~__c✓=-• ~c,· ~A~•~•-~-------JRILLING LOG ). A.'.lDC.,:SS, sy-. p-1/ /3 ) '3 / ,'ZQ, b«<==- 4. _':"OP~?..APHY: dra· .... ,·-1alley .~0illtop, flat {circle o:-:-;:j DEPTH fRO-'.-!--TO FOR.~~TION DESCRIPTION 5. t.:5::: O? W2Ll.: Pc1c1: DATE, 9-?-rr) 6. D02S ':':HS •,,~LL R.EPLl\CE AN EXISTING WELL? ;U) 7. 707,;_:., DEP7~~ ,;) ct/ RIG TYPE: OR H£THOD: t?t'!/'d< 8. ?O?_..,_;::-ros SA.:·:?LES COLLECTED: YES ~o L---"" Depth Inside Dia. ?=-o~ to ft ___ _ Material !re:: tO f::. Wall thick. t:t?C or weight/ft. Method ----- If aaait1o~al space is necacd, use bacK of forrn De? th Dia. LOCATIO~ S~ETCH Frc=i ___ to ft ___ _ (S':-.o·J clist;,.,;-.cc to nrn:::bercd ro:id.<:, or o:.hcr C:'? rcf.;:~cncc points) Size Material ?:.-o~. ___ to ft ___ _ 13 3 3 ~ !E!..6(gp:':'I) : _____ .HETHOD OF TESTING: ___ _ 1--'-,-?i..::-'.?I::,;:; o,..·;..~R LEVEI.: _______ ft. a:t~= _____ .hou:-s at ______ ,gpn. !-=I-c:::.o?.::--:xrio~: Ty?e _____ __:J\.mount _____ _ 18. ;;;.T~~ QUALITY :e?;___ /j-o 1.-&-: ,-.:..-_~_.. ••• .::.. •• I?<..;":?: Date lnsti!.llcc!~-------- :-..::::cc:-:.:.:.z::o,;, 1 ex s? 2 l . ;·'c-=c~::cc:C.y ~1,~, Lh~:~;,~: '""~' cocs:cuccco ic ecco:ce.cc•, .,, th !I .C. 1:01] Cone ttectioo ~~;u:~tio~s a~ci St~nci:1rds a11d thal this ~~11 reco:.-~ is true a~~ cKil.Ct. ---~.( -~½~a (-►~---~--~,;r--~'-c> ,,,,..-·1 , .••..• ,.. I.. .• , ...... , •. i). ··"···'· ..... ,.,. •..: .. -~ •.:'-l=--~ 1.JD:~<-q' 5,::::.:~iL ,1:.-i0.:.:.::~ :.,:, -:;:-L,·..::~::·~·~,::.c:r /o D '/. I .. ,/ .· --~~/ ! ,: I __ ;;·:.r;,,l:Jgic. Log v.-:::-- GROillillJ·;ATE?-. SECTIOci J..... b 7G3 Field ___ _ Office ___ _ 1 · ~\ t;"·~· ________ Date 9 -f--fiJ Couilty c/~,t!/1 . 0 ~2. ::'.c::' 7 own __,_r:ff-~___,_/7/o,;.c...___· -"-/~?'-?"-' .,_? _ __..,/c....--:::z.-,<=l.-'"'-'·-"'£"'--,<CL..; '=a~«"-'='----'''-=,._,,=--=c:._=-.-- USGS, ____ _ 1 Cc:::::-~/:~~f~..,,..~~"o--~f'.~:J-s-,,.,_,,F-· -'-"'==---~=------Driller _______ De,cc, Drilled ____ ..:__ ;;. 'i'.._' f', If ' Cased to ___ ft.; Elev.'--_ft. 1_,pc~~~i~_ft.; Diam. ___ in.; 1!:~~::5s _______ Elec. Log __________ Ga-.=> 16g ________ _ I I I I I I I I I I- I /IJ- /i-,y'. u ~ ' :.._;;:-7. Description I I I I .. I I I I I I /. /, 0 i I I .;l.,_>, 3 I I I I I I I I I - I I I I I I I I I I I I 1: I / .,,I Ci:,n"RAL L~50:t:\TO?:i c'.E:?OR.I ( --... ---.. = :... :..__.J Tas::e. ·--------------------?:-:: . .o.o: T:sr FOR C0'1SIITUEcITS OR PROPERTIES . .\.S T~llICATED. G?.C,:,:-.:;:.:.0.TE:\ SECIIml, RA.LEIGH N. C. REPORT NIALYSIS TO: CHIEF, L-...; iX ~ .-- c'.::.c:.zlinity (As Caco3) < / to pii 8.3 ....•. ···~·-----~mg/1 to pH 4.5......... .3 mg/1 .-'-. .2.':.= in l! ~ - • . . • • . • . • . . . u g / ! -------- ~=senic .......•...... ________ ug/1 3i=a~ba~2t~ ......... ----~----□g/1 I 1 ::.:::, · 5-Z)ay........... ng/1 -------- 1 ~ c~~)~n2~e ............ ___ ,_·_/ ____ mg/1 !)<: ::·,~::=id;,............. rug/! ~ __ _._ ____ _.c , __ ::-:.~:o= (Total MF).. /10021 ------ ::!??er ........ ; ••.... _· _______ ug/1 ~ :::::: .. ; · ;;;;;;: : ·JQ ::; : .•. :J.iG, ..•.....•.•... \~) mg/1 I L.___1 :C:e::-.:::oes,; as C?.C0 3 .... __ 7..,_L ____ m.6 /1 ' Z :, e = ~ ~ ~ s ~~ r :>o na t e ...•. ___ (:;_~-'-------'mg/1 --,................... ug/1 -------- _a.s.::................. ug/1 -------- ::..=..:-.5~u2se............ ug/1 -------- ------· >:-::-:-: •J z y .............. ________ ug / I Nitrogen Kj eldahl. •..•....• cg/1 ------· Nitrate & Xitrite. t:17,/l -----_.C pH Val·-1e (h'h2n ~nalyz ed --=c...:.......:_ 5,2 ug/1 Phenol .•..•...•..•.•. ______ . Pr.Js?horus. To~al ..... ------· .:.g/1 rq,/l Potassium ............ _____ __: Soecific Cond~cta~ce (cicrowhos at zs 0c) .. _____ _ Silica ..•............ ro.g/1 ------· --::.-;/1 Sodi= .••.•••.•.....• ------· Sulfate ..•.•.•......• _____ _..: r:o.;;/l ug/1 Zinc ..•....•.•......• ______ . r::.g/l c:.;,/1 R.~2.rks: C C Q?: C C I L.....-' r--L..c r--I_ t L..._ C C C C 1------------.:........._ =°: ?. ~~;r::~.L·\B USE t~-,-~,,-!,,'Ell RECO:=tU J.J( DJ VI s I ON OF ENV r RON,"',ENT AL MANAGEMEtlT, G~OUND',IAT'::R SJ·cr I ON // (. O. DOX 27687 RALEIGH, N.C.. 27llll ( t ... /.,7,_,;, t{;/<. !)ll£G. ·No. h"ELL CONSTRUCTION -,.P 3 l DRTLLI:JG CO~:"I'RACTOR 1.: I I I I I I I I I I I I I I I I 1, 1-iELL LOCATimi: (Show sketch of the location below) L · f;e.z:.res t Town :, __ t_/..Lf'Z.s<-:'-,:,c,?c!J~· '2..~fc_../,:;,o:JLiLC'"'-'~=--'-,-----="--=-____ Coun ty: l-✓£ L Y&-/·13}? Quadrangl: No. L__ (, ·2 a (~oad,Corr.munity or Subdivision c1nd Lot No.) ij .2 - one)· 5. USE OF WELL: ---'U=;:~:..-c:"°'~q_r-'.: _____ DJ\TE: /-9 DEPTH f'R0-!·1--TO JRILLING LOG FO:l.'!ATIO;i DESC?..IPTI0:-1 6. DOES THIS WELL REPLACE AN EXISTING WELL? __ _,/~L/==c_~l~)- dg,d d --G-J: _JQ,-,.-17. RIG TY PE OR METiiO,, oo_, __ /'ZM;_,=_c__-_✓_/_L_ 8. FO?.:•lATIO:l SAi·!PLES COLLECTED: YES • / 7. TOTAL DEPTil: .£..--::/-,,,_ / ,--;:;? y / Depth Inside Din. to ft ___ _ Miltcri,1.l \,,,'all thick. or weiqht/ft. Method to ft _____ _ type Depth Dia. Type f. Opening to ft ____ _ l-!t":-GRAV£L: Depth Size Material Fr-o::i ___ to ft ____ _ 14. ST,\TIC W,\TER Ca!>ing is -,/ LEVSLz;?</, /ft.~ -~·UL-tt. nbovc l;:1ncl ~urfc:c,c ELE:V: e-:-YIF.:LD(gpm) : ______ METHOD OF 'i'ESTWG: ____ _ i-c·: PU;-:f'ING WATER LEVEL: ________ ft, a~tcr _____ hours at _ _,_ _____ gpn. i-r.· C:iLORINATION: Type _______ .Amount _____ _ 18. \·:ATE:R QUALITY: {~,,./ .3•.~-(.) TE:!-'.?ER.i.TtiRE (0F) C., C Ty~~ _______ ca;:;c1ci ty ______ (gpmJ Hr ___ _ :-:.:1>:e ____________ I n t.1kc Depth,_ ____ _ Airline Depth ______ _ ~ Ir acc1t1onal space is nee=co, use nae~ a: ro.:-::i LOC,\TIO;l Si-:£7CH {Sho•.., distaricc to nur.,berc<l roc!.C:;, o~ othc:' _:..J? :-ei,;,;r,•n::e ?01:-.<;.s) [!0 J I /} " LJ ..:.. l.J f/3 /DD<i, '::, '3 /t70 ) 20. ll,\S THE o~-~iEH ll!::CN PROVIDED l\ CO!''; OF 71!1S RECOiW At:o InFOil:1,?:D OF THE o:,p;,il.71'".E~:J:s R=.OUIR:.::-:z~:-rs A:;o IE:co:-::•IE,.Di,T I ON .s? 21. I\C::•'..:,~,s __________________________ ----··-____ _ ;: 2n h-::l·'co!"~; P . .:-sulLltio:i'.> GROUXD!,ATE?.. SECTIO:•i r 1 field ____ _ 0££ice ----uses ____ _ I _G'c.'::ce::~/_?_,_1~, ___ d~~~-:;~·r-/l.='=4=~~1~/~ ____ Driller. Q.,;, > /j,, ,,..,__,_< Da:,.c.e ;:JC.._,, ~ / __ ,,, 21 I ~=~t·~---~-a~_ft.; Diam._~"'-'~_in.; Cased to ___ ft.; Elev. ___ ft. '--'-::::.::53~ _______ Elec. Log ___________ Ga,_,::1 105 _________ _ c.bovc HSL I Deo~h (f2at) Thickness :--~£J~, ~-· -_,(7~1/;-'--'-',)-",,.1-_,.j~~~~ J:~7------,-r~·=~~" !~:-0 r-;-! --=--.A--'=~'-'==':..::::C...) _-- Description /6J~ o"&_//, ,A ) (7 /;,., =-,C,...,/ ~ /cf' 0 I I I I I I 1 I I I I /7 . ,, ? ~/-f/2~_/ 1/r~s· G3 /LJ,7.:/) ,.(___5-, ...,/,k, a '>-L {;e;,1. / I '-./ I I . I I I ------------------------,----r-----t--.--------- 7 C>ii'.__;i :+' ·2 'I. 2 .. I l I .· - . I ! I •"•'••·•-_,· ~ .. ',,../_ ( Gri~ Locat:!.o" /._. &, 7 6--<'/ L':\ b . Sc~ N uc:b er ------- :;,,_;::~ Co:2.ectedJ-'!-i,FO Tir:!e:___. _____ By: /~;_, /~cfoo{/ 73 1 1 :.02~:io:: or site ;?J,,dC'-:'.:=__:,_,;;,:;'c'.c.__4"-4'--1":,;~?"'--""'_"",..-';/lb-"""-;--;----,--------------- ~~5c=:?~io~ of Sampling Point_---'-p"-'ti=1~0-"--'£~--~-----------------~---- I ?.=-=.:: :-;:::; ----;:::--:--~-:-----:-:-=------------;---------------------(?=?in g Tirae, Air Te~perature, etc.) ::-:-:-3 .! ',.!.LYSIS I ?:::.-____________________ Odor _______________________ _ S?e~-Co::d._=~,S-=-_u ____________ Appearance_~-~--------c------------- Tas::e 1 ::.::p . ______ oc --------------------FOR cmiSTITUEIITS OR PROPERTIES . .\.S I"'llICP.:C:::!l. RE?ORT .?.X . .'J.YSIS TO: CHIEF, SECTION, R.~EIGH N.C . I 2.-::,·_~:::,-:_:-=3 . ;:O.c--.2.linity (A,; CaC03 ) -</ I I I I I I ' .x ,-, __ i__; 1y ~ .>(, Co prt 8.3 ........ •---~---c,g/1 to p:l 4.5......... '2---rog/1 . .:..2...=.ir..u:::i............. ug/ l -------- ;_:-s-2"2.ic ............... ________ ug/ l Ca~bo~ Dioxide ....... ________ ng/1 ::,2.c:rid?.............. S sg/1 -------- :::.:,2.::.::o= (Total ill').. /100:::l ------ ::p??.r. ; ...... ; ...... _·--~-~--ug/1 ,....---<-·= :--=-:::..i.C:.e •••••••••••••• ~✓ rilg/1 -+---~+--~ :·:ss:,lv,,d Solids.... 3/S □g/1 1---~---- :=-·.::J-ri.:i~: ... - . . . . . . . . . ~g/1 "'-==--"'---------' ::·-0 ~~---as ,",cO ) lLQ "/1 -~----~-' ~--3 .•• ·--~.l~----"'" ~e.~~~;s;~rbonate ..... ___ /_3_9 ___ ~1cg/l --~----............... ug/1 -------- _:::...::,_............ .. . . . ug/1 -------- Nitrogen Kj eldahl. . . • . . • . . . " ---.,...,--',--' sg/1 Nitrate & ~itrite. ---+---+--' P" \'2h1e (\-:ocn a:ialyzed .!./; JI -f--''--'--''"+-- ro-z./1 P~enol ........•....•. _...,._-""---~ ug/1 Pot:2.ssiUw .... ." ...... . s~ecific Co~d~~La~ce (~crowhos a.t 25°c) .. Silica. ...........•... Sulfa.te ..........•... r:.g/1 ------~/l ------- r,g/1 ------- r::.g/I r!'.f_;/1 -------' ug/l c,;/1 C2lc~1.12 .•..........•. ______ ...: Y.:.2.gnesit2 ........ ~ .. . r::.-,, I I --------= Re..=!ark.s:: D D cgi D □ I I I I '7 L.J r-1 L...._; D □ D □ I I I I I I I I I I I I OEVELOPi·\ENT OF (NV[RO;,..;'-'c·nAL '-\t.'/\G:·1:::n, G~ou•,o,.:,TE( -i::-crroN .O. BOX :?7637 P.AL::JGw, N.C. 27611 I c·..<.YR.F.c. ·No. h"ELL CO~ISTfWCTION PER.'1IT NO.~ i/ 1. ro-=:LL LOC,\TIC~:: (Sha·,... s~:ctch of the lo:::.::ition belm-:) /) /' _ / ~~e.?rcst Town: /t-C-[~_,.,..~//n1/'-/ · ,{__/ Cc: Co'..!:ity:_~,-~2?:=~-==-~-<=~=·~ .. =~·,.__·_··_· ------'-----"£_/=• _·J_e?,:;,_/ _ _,__,__;,__-,,_· ·---~-~---------Quadrangle No, __ L-,-~c~~-~z_e-~_s-____ _ {noad,Com.munity or Subdivision and Lot No.) 2, c·,o:e:~,--L/7-_,__,/,<-.<t""'---:;e=5=~-/c_;0,_--'-"'7.,_f.,_f?'-"• J"', __ . ____ _ .s;, /2/ I 6 .; ~1'<<-r'u1r?1J 3. ~D?.i:SS: -:.. 7OPCGi'v\PHY: C.r-aw,valley,slope,hillto;ift§Ycircle 0.'1C) -/ ('.' c .. , 5. US='. 0? WELL: /<..g% DATE: 7-cz _ ifL' S •. DO:C::S THIS WELL REPLACE Ml EXISTING WELL? __ _,,fV_,::_:U::::,' __ RIG TYPE OR MET!-!0D: ~ 8. ?'O?.:.,.A.TION SAf!PLES COLLECTED: YES NO _______ _ Depth Inside Di.:i.. ?ro::i to ft ___ _ Haterial Dcpi:h Dia. Wall thic%. type or weight/ft. McthoC. 'l'ype & Oper:ing .JRILLING LOG o::?T1! FP.0-:o!.--T◊ FORMJ\TIDN DESCiUPTION u--d- 3 lt aoc1:1on;il space is n~cucu, use bacK of tor~ LOC;..T!ON SKETCH :~o=i ___ to ___ f t ____ _ (S'.-:o._,· ciis~J.::,:e ~o nL!=.:iert::d roads, or other t:..:tp rcfercncl! poinu;) Depth Size Material ? ro::-. ___ to ___ f t ____ _ 13. ;;_.;72:t Z0!\2S (C.epth) 57,;::-rc WATER Casing is 1."'5"".-'il~LD(gp:n) : ______ METriOD m· TCST!NG: ____ _ a::er _____ hours at _______ 9po. i:-7-:--· c:-:::.o?.n~ATION: Type _______ ,Amount _____ _ !S. ;.:.;T;:R QUALITY: {~-?.7 /9L: TU1PER,\TUR£{0F) (.'(; I ~~:':C:?...".A::21-;'T PL':-!?: Date Installed _________ _ I I I • : ~ e _______ Cap;ic i ty ______ { 9p:;1) l!P ___ _ :,:2.:-:e ____________ 1 n ta):e Deµ th,__ ____ _ ~c-:-::..\S T:-!Z oi-1r;2R 3~£:-: PROVIDED :"'2cc:.::,£:rn:.., ro:.is? ::: ::::-:-;~r'::~)J ?.es;:.;lations ~~11 Construction lJJ;.l"ll!U:·!.t.is"c Ul' ~:ATL'RAL A1'!D ;::coc-:o;-rrc RESOl:--:=tc::s GROU?-IDHATER SECTIOci 1xT I :>t:}~fl.:,~o£ic Log. · ~\f!ll ~:o~: 1-7Fie~d ___ _ '\(. ~--· -Dc,te 9-9 -Jv Countyd,-z_,,~/ / · ~~~~-c ___ _ I 0:~ ::o--r:-,-,:o-,-m-_-_~.-J/:'..!.; _____ ~G~Ln1/-:::/'...J.1~)~7 ___ -L//L-f,c::_:.::. ,..?'-'-'"---' 4&-=-<:::o~==~~=---=::=----I c·.:.:e:: . ///,,.,_, Driller {1_, )4--<-<--"-// (/ Dete Drillec_.:.._9_-----'-9_,_fO_;____ i·3, ft.; Diam. Cased to ___ ft.; Elev .. __ f.::. c.bOVc! HSL_ I Description Deo~h (f26t) Thickness •---/-t-?J-.-,(-i%,--=-:--'-.~---,-:\r'.-;--,.....,< ___ /_:-----:lf-fr-:-+1-;-:+1-,/-~~--ee_~---- 1 d: ? I I I /Lc1l ..L tS: /__/).,-.., ~ .I I I I I I -&.o,.,.,J r-1:-/2-, / I "L l, · ◊ r}/4/· d--dr)/Z,J" :Jc. J -~ ,-l"'. . / y /.3 / / j''l 32' (_:::i J/ (~./) I I ' / I I l I I I I .- ~-zf..~(.-~T-~~~9-~~--,--------,---i--+-----~:.:J !fn.,._,__. -/'Jc.? I; I I . I I I ·-· .. .•. I I I I - l I I I I 1. I /VJ C:C:e.'TiL-U. L'\?,0?~'-.TOJ.Y ?Z?O?,I , ' ' Grid ·Locati_o,i L 0 7 (;_. -S L7' b. ~a..J.. !iu=.ber --------..,.1;) 3Joo?...-7 z.... . :::a== C CJ 2.2. e:c t eedJ -9 -_.ye) Tiroa,:,_ ______ ily :_...c.A.....;..a=c..~=...=aoc..·_,-0-"'. -L./_'.;.1;_~~·=0='.(...,-\____;-==---- I.~: 2 :::.c:: or site /c,,f.i/,c;.· .. ,,_.-"''-,-----"'>!;J..~"':,1-'TJ-:ro::J,"""4<'-"'h,,__---;-___________________ _ !;,c3.::-::.p ::C.a:i of Sa;;ipling7roint.__~f?"-'-'Q'-"-.:..,~..,..,,""'-. ________________________ _ I p:C: ______ 1 _. c:; __________ Odor __ ---,--________________ _ S:;::-;:•=. C:0::.:::i. -11 Appear2.i:!.c.e -~----'------------------- 7as::2. ·-'-------------------- -:>7 7.:: :----·--?OR CO:iSTITUEtITS OR PR02E?.TIES AS i.:mrc~.T:':D. REPORT ;.}:OJ.YSIS TO: CHIEF, I I I I I N.C. iX i...:.:Sliuity (As CaC03 ) ·. :c p"ii 8.3......... -< / rog/l --------• X: ;: a ?=' 4.5......... 2 c:.g/1 L--_.:_:_:.:::;. :i...G. u::i . • . • • . . . • • . . . ________ u g I ! ;._: s :=tic ............... ________ ug / i 3~~~=bu~a::e .......... ________ □g/l C~:-~:):t Dio;.:iC:e........ ng/! _______ _c :~,2.::-idc,............. _J sg/1 ----'=-----1-·. : :o 2.::.: o = (Total MF).. /10021 ------- ::ppeer ........ : ...... _· _______ ug/1 -::-·2.:::!.C2.............. fr-----~, "2.g/ l -,-'------\----· ::O:,ss::>lv,,:i Solids .•... ( \13) q;/i -!--\___../~~"-.-"--- :: :. ·~ :,:-i~,: .. ·........... !!:!.g/l --------~ · -"~, ---ar <.,-,co ;,7-7/1 --=. -..__ ~.=.. .> _, •• 3 .•.. ___ lc..=.v ____ c..o - I :::z::-:::;ess, "/ .__£_-!::;:: C2.r:Jon2.te ..... ___ ; _____ c::;g/1 I I I ---··· •·. • .. • • ........ ________ ug/1 -=-·................ cz/i -------- :.:::-=:.:::-y.............. u5/l -------- I a,--.". s-'I·" "·c _______ .::, ___ 1_1 . ' -~ _, -'"'·: • .... :J_1 _ _\ __ _ Nitr-ogen ,,,,,.-·., ~jeldahl .........• ______ ....c \mg/1 / ;ni/ l ~Jitrate & Xitrite. ----'----CC p::! \'2.lue (\s'hen 2:12.lyzed'-----i----"-'-'-'-I~ c; i . I I ug/1 P~enol ...•.....•....• ----'---"---- Saeci~ic Coni~~ta~ce (~c,owhos at 25°C) .. Silica .......... · .... . ng/1 li:g/I ------- rag/1 ----------' Soci i~ ..... · ..... -...... cg/l ---------' Sul£2te ............. . ----------' mo-'r c,I - ug/1 mg/i. r:ii/1 C; ! -, r . LJ D ~ D □ I I I I l ! l I D □ D □ .... ' I I I I I I I I I I I I I I I I '.{ELL P.ECO?.O O!Vl':,ION OF ENV IRO~:-'.C.NT AL MM!AGE~ENT, GROUtiO'r/,\TER SC CT I O."l N.C. 27611 c··. ( 0. BOX 27687 -RALEIGH, . c. OR::c. ·eo. l. h"SLL LOC,\TIO~:~ (Shen,. sketch of the locution below) Nearest Town: T?i--c-~~ 1· ,..,/· d-1()-, ..__ rL/ (_,.,. WELL CONS'l'RUCTION PEP.HIT NO. ' ...::-5C.+~Z...,-,---L.{..;'?c:;Jz__,(L,..j''-c-·.,_;_,?"-~~-,---,--;c:--;:--;:-::--;------·Ouadrang le No, __ L-__ 0,c·~·~7_(Z,~1"-(_=---'---( ao~d, Co;;i..~uni ty 'or Subdi~ision and Lot No.) 2. o:-.o;zn, /l/1 ,::+· w,""z,O L.--_ · ). ADDOU:SS, ...{.:,,/-c/",i 3 J ~..,-,hwo 4. 7D?OGRA~HY: C=aw,valley,sloµe~lat(circlc one) s .. US£ o: WELL: h:::::1 ;-,'( DATE: 2-c; -J-r) 6. D025 THIS \.:==LL REPLACE AN EXISTING HELL? i-? {) 7. TOTAL DEPT:!: C) tr RIG TYPE OR METHOD: 1:ltr 6. FO?J·L-'\TION SA.'!PLES COLLECTED: YES NO £_/ Depth Inside \,'all thick. type Dia. or weight/ft. Fro::i to ft ----- -iD. GROL"?: Depth Mntcrial Method Fro~ to ___ !t ______ _ Depth Diu. 'l'ypc & Oper.i:ig DEPTH FRO-M--70 10-£,,,: IJ,,-7 Y_., ..JRILL!f.G LOG FORH,\TIOS DESCRIPTION Ir adait1o~al space is neeaea, use oac~ of ro=Q LOCATION SKE'i'CH Froioi to ___ ft ____ _ (Sho'.J distance to nu;;-.bcrcd ro.1d~, or o-.:.hc:: t"\.'.lfJ rcfcrc~.cc poir::.s) "-:l-?....-G RA \SL: Depth Size Material Fro:-:i ___ to ___ f t ___ _ 13, h',\TE:R ZONES {Cc?th) : __ ~'-"=-:,'-t~'._J_1 _________ _ 14. STATIC -,, b h'AT£R L!::VEL,'~ _; . ..)ft~~ ~ ~ '-~ L-casing is ___ ft. above land $Urf<.:Ci! ELCV: ~ YIE'LD(gpm) : ______ 1-:.ETHOD OF TESTING: ____ _ uftcr _____ hours at _______ gp~. n-:-cHLOiUNATIO:<: Ty;:ie _______ .J\rnoun::. _____ _ 18. ~:A'iER QUALITY: &~ l_.() TE:1·\PERATURE(of'L.Lf. Type _______ Capac.i. ty ______ (gpm) HP ___ _ ,\lrlinc Dc?th ______ _ i-o-: . ii,\S THE o:,Jl\ER BSE:,;" PROVIDED ii COPY OF THIS RECORD ,\HD 11;:·oR:':r.;:, o: 'l'i(E o:;PAR"i'i·!E/:Ts R£QUIP.S:--:::::Ts i\.:;o ,,.z.co:.·,;.-.::::: o,;T 10:-: s? L·l·:·· 11.2:,._,·,~r. ----,------------------------------1 Cc-hcr·t:!:i/ c..:~c..:..:y ::.:1;1:.:. thi.:; .,_-~11 .,,.,1~, co;:.:,t:·~c::..cr.l in a::co::dc:,;::..: ·.,!th ::.C. l~cl.l Co:,s;:.cl!ctio:-i Rcg:.11.'.ltio;-is .1nd St,"\:-idu:-c!:; .ind th,1t thi~ . .,,-ell rccon.i is t.::-uc ar:ci c:-.:.:ict. ,,.----~\k~e"~-:, ·fi,,,,, <c ;-J ,~ %"'.:/·(__Z:~ ~ -.rv (..)-,! ;{~•✓i.":'.>( O!(J:·· t;l:h:.~i'::. o:·iui::.:1 LC> r;,r, ,:"r•i,•• .,,.., ~~--·- I ___ DEPART::lENT Of }'./\TL'RAL i.:':D ECO?,:O'.:IC PJ'7'1l;?.C:S ! ''·it:o::>c.'.lgi;:: Log ·, ·~og c;~·:~ _________ Date ';:-9~,IZJ ) __ ., •· -ca,~ r, / /4' / /:3 3J I -~--<--.. , -••U :+::ecL .-:: "::: /! f,., ,::fr,;:2~__, ,Y 3 J-' ft.; Diam. in. ; Cased to __ ! !{ell (~o. !.cFSFiel.<l ____ _ Office -----[SGS _____ _ D2tc: Drilled ft. ; Elev.'---_ft. c.C>ov2. HSL I ct ~:i.:::.5:s ________ Elec. Log ___________ Gar:::.::2. log _________ _ Thickness (feet) I I I l 1--t---- I I I l-~--~-----;-1---:----t----- l I I ···_· -------~! ~-r---- 1 I -~ br-~ I -- 1-· I I . .. ~ / -Lv.-Y f~o-,.__ ' l -, --c·-'( ~).S,J t'.u I I I I I CE:ffR,\l. L<\BOR.'-.'i:O?:[ P.i:?O?..I Griq ;Locatioc: L (, '7 (~ -c (,u~·~ ( ~~ t,u::be,:: · i .;d3_J'_o_o_Z_7_/_ I: :J~:c ,::::,llectc,dJ-9-'fr, Time'-----'-------B.y:_,fl--=q'-"~-='-'--'=-=<-,,_/.::..._..,,,,l,,t,t,tl-d-<,,'--'''------- 1-- 1.,-.\ :.0=~:i::::: or, site ..},µ""/4""-i""",""'r, -""A~.1.=<'_,,'-;">"'Y7~-~=<~, '"'-'-':;-c d.,,.-/----,,----------------- I I I_ I I I I I I Desc~~?tion of Sampling Point._~?J.L..~Q..,;,_.dd~K""-~cf.,_. _____________________ _:__ __ _ ?. ~ :-:..:: 3 -:-::---:---:::---,-:-:::-'-------~--------------------(?=ping Tine, Air Te~perature, etc.) ?"-_____________________ Odor _______________________ _ S?2.C. Co.::d. ( 0 A~pearec:ce ____ '7'"__________ -~~----------------- :;: =-"-? . _______ oc Tas~2 -.,-------------------J;-:~:::-. --•P -:::sT FOR CONSTITUENTS OR PROPER.TIES .i.s 'i:lillICXc'::D. RE?ORT .'.lL'-.LYSIS TO: CHIEF, [sz:: ;.< .~>:.e::.ini ty (As CaC03 ) co pn 8.3 ......... _. ___ .L:.~/ ___ ng/l to p:-i 4.5......... 2.. og/1 ' L_ ;2=inec,............. ug/ l -------- I L____; A~s2~ic.............. ug/1 --------:)< '-'---3i::2.rbQ.-iate........... ng/ l --------,---: L__!. :::·JJ, 5-uay ........... ________ og/ 1 Xi :--C:2:~:,:on2.ce............ _,,:_/ ing)l -------- i i Cc..:-bon DioxiC.e....... mg/ 1 -------- lK'. C~lorid~ ............. ________ mg/1 r--_,_ :::~::.i.forn (Tot.sl ill").. /10021 ------,--, L___; :'.:-O??"r. .....•. ;....... ug/1 -------- Nitrogen Kj cld3.hl ......... . r;;g / l ------..: lJitr2te & Xitri~e. r:J?,/1 -------' pH \'2lcie (,,hcen 2.n2lyzed --~~--j,S Phenol. ...•...•.•.... Pot2ssiw:: ............... . Sc2.cific Condacta~c.e (cicrowhos 2t 25°c) .. Silica .............. . eg/1 _______ , r:og /1 ------~/1 ------- ng/1 -------· Sodi=··············· ------· q;/1 Sulfate ....•......... ------...: Bgi l ug/1 D D @ D □ □ l I L_J I/ ~ [J D L__; ·-=:-·2.::.~C.e ....•.......... ________ mg/!· I ~: '.:;:.ss:::,lv,,d Solids .... ·--~_r;'-'~----CJg/i Cele:.= ............. . _____ _: cg/1 D □ c3/l R=.::::.arks: ::.~=-~:-..2.ss, I,! :--<:_,i -~:o;i C2.rbon2.te ..... __ z_C:, ____ mg/ l ; -~~::................. ug/1 I ..__: -==· ................ ______ ug/1 : :..::.:'.:i...:.::i .......... •·,•.. "...!g/1. -------- 1 · ::.,,~_;;;.:i2se............ ug/1 .~ -------- ~ ~:=::-:..:.::-y ..... · .... · ..... ________ ug/1 I I 0 ---'. · · ·1-cl.~ ~0 .,::._ =--:::: :, .• . . j.,} -I ~ ' -·,-, .. -ii/\ -V.;. -·•-'...:+--- I ' I .. ·i I I I .. I I I I I I I .-- I I I I· I DIVISION 9c:; I. ENVIRO,'-::-',E~lT,\l '";f,'!A:;.::~=~n I G~OUt!D,,,\TER y:cTION . BOX 2/687 P.Al!:l~H, N.C. 27611 ( C. kEG. ·r,,;o. h"ELL CO:ISTRUCTIO~ PEPJUT t/0, -I-/ l. ;,::L!. LOC,\'i'IC~:: (Sho•..1 skctC:h of the loca~ion belo·.,) 2. j-v c., .. C.=a.,.., valley, slope, hill to;,:> ~ircle 5. css 0? saw., _:z:;,__.c·..,cc1.__--:l...,____·· ___ DATE, 9-/0 -fe 6. DO~S 701S ~~LL REPLACE AN EXISTING WELL? ___ ~u=_,u"- RIG TYPE OR ,METHOD: /-lvc.UL jJ NO'-"' 8. lO?...'.J_;TIO>: SA."l.?LES COLLECTED: 3,3 1 YES Inside Wall thic'.-:.. type Dia. or weight/ft. :"rc::i to ft ------------ Mot.:cri.:\l Method to ft ______ _ Dia. 'l'ype f. Opc::ing D£PTil FRO;:r-TO .>RILLING LOG FOil}L\TlON DE:SCRIPTION <H;..f er-J;;,,..f,_~~ d:: Ir <1c~1t1onal space 1s nceacd, use nae~ of ~arm LOC,\TlON SKE:'l'Ctl :re~ to ___ ft ____ _ (S~o·-· d1st.:inc:c to :,:::-.~ercd ro.:idt.:, or otl1cr C\.'.lP rcfcrc:i.ce points) Size Material F ro:: ___ to ___ f t ____ _ , , S7.\7IC ~,\.'!R Ll"VEL$ 5ft Eovets • oinff'l'f~ g: -· __ ._ "loW'<[L 2 ------- Casi:.; is ___ ft. above lo:id ~urft:ce ELEV: /oo.S-1?"'7'"' i."IEL9 (g;:,::i) : ______ METiiOD OF TESTING: ____ _ ro:-·?u:-:.?I~:G W,\TI:R u:VE:L: ________ ft. a~te" _____ hours at _______ gpn. 7ype _______ Arnount _____ _ 10. :-;,\:';::\ QU/J..ITY: __,,C~~-2c·~?~'---'3U~·-· _1'.E:MPERATURS (°F) /,;"' l_ ~'.:..1 :-:c ____________ ln t.akc Dcp th:_ ____ _ DEPART:·R:N:!.' O'f }'.ATL'RAL A.:\'D Eco:-:o:-ac RESO ~7,CC:S GROUNDWATER SECTIO,i Log !\ell to .. ;.:rfb Field ____ _ Office -----uses _____ _ I 0:r.:e= /'.?i._ c:: G ~41Vl'I, Driller (1; )$ ,, ,,~ De.ti'! Driller .; . 3 , c) / r/ . . ZJ 9-/0 -r'--' ,~·-'Ft!, :J . · ft.; Diam._'-'f-,'--_in.; · Cased to ft.; Elev.'--_ft. :t;:i:z.5s ________ Elec .. Log ___________ Gar:::::i:::.2. log _________ _ I. I I I I I I I •• I I I ·u__,7 , cl L-J ;..:r en/)7f -- Description f:" ----,;!· ,J J..'.r) I I I I Deo.th (f2ct) fr or:! to 0 t=· /3 ,,, /3 I 3 3 -I I I I I l I I I I I I Thickness (i2et) I ?. =-=-=-= :, .:i ·---==--------:-=--------,---:--------'------------(?L2?ing Tioe, Air Te~perature, etc.) ::-:-=-3 .;.~.-U.'::SIS ~-Odor I -----!-,,..->, ------------------------ 57-=:r:. C::>=:i . __ .,.6 .... c~u __________ ----'Appearar:cec.._~--'------------------ Tas::2. 1 -;:=? · ________ oc --------------------?:..::::.:'::: ::-:::sT rOR CO/iSTITUEcuS OR PROPC:RTIES • .\S :i:cillZCP.:CC:D. REPORT i0!.U.YSIS TO: CHIEF, SC:CIIO/i, R..UEIGH N.C . . -~ ... ;:,,1,-,;-~, ('s ca~o) .-...:.,. ___ u._ L_J n Iv 3 to pl:! 8.3.. .. . . . .. ,,c/ □g/1 -.. 4 5 _____ /___ / l ;: o p" · . • . • . . . . • . -< mg _ , __ I._. : : /. _:...:_~iht.!3 .......... •.. ug/1 -------- _:....::: s :;2ic. . . . . . . . . . . . . . ug / 1 -------- 3:.:2.r,,.o::a te, .......... ___ -< __ J ___ ng/ l I ,-- ' I __ : ., >( i 1· . . --,::;..:::io::i Dioxide ....... ________ filg/1 : x: C:':l:orid2.............. mg/ 1 --~----- •. ; :: . .:.:.fo= (Tota:l MF).. /10%1 :~??2r ........ ; ...... _· _______ ug/1 I I ·: ·_.-2.::::!.ce •••••••• , ••• • • r;ig/ [ \....____; -------- ; ;;{: :·~ss:,lv,,d Solids .... ·-~(o_') ____ □g/1 =.~::.:i::..e.sst ::c,:: Caroonate..... 33 mg/1 -------- I ---··• - . - - - •.......... ug/1 -------- --c..c -••••••••••••••••• _______ ug /1 :.::::-::::...:.=i.............. ".!..g/1 -------- ·::~:-:·-=.::y .. • • - . - -. . . . . . ug/1 --------I Ni~roge~ /----,_ "jeldahl...... .. . . / -, rc.g/1 l,it:-ate. & );itrite..--'--/~~\-.:.../ ...:r:,_5/1 pH \'al:.ie (\.'he,n 2nalyze.d / /../. D/ -j----+- P:-'.er:ol .............. . J ug/1 ~= Pf'.os?horus> To::2.l..... -.:.g/1 _____ __; Potassium ........... ·-------'~/ T_ Soicific Condacta~ce (dc,owhos at 25°c) .. ------ Silica .......... .' ... . og/1 ___ .c.._ _ _: Sodi= .............. . _____ __; :::g/ 1 Sulfate ......•....... ------□g/1. ug/1 cg/l Y..2.gr;.esiuB ........... . r:.'l,/1 ------' r.. -- D D fg] D □ □ D I I I I D □ D □ I I I I I I I I I I I I I ' ·-· I ··- I I \.'ELL RECQ;:::O NOR.HI CMWL!N:, (J~?/,!-!iMf.llT OF N,\TUR,\L R!:SJ;;;.,,c.:ES l co:-t,'-'.UNITY DEVf:.L0f'~•.~::1 DIVISION OF ENVIRON.'·IENTAL M/\.NAGE,~;:Mrl CROu~;o·nATER SF.CTIO:-l r r ( 0. BOX 27637 -RALEIGH, H.C. 27611 { l•;LLL CONSTRUCTION PSR:·IIT NO. 2 • o· .. ;-.:::rt : __ .....<ij_,.c:1/,'c,rc...· ,,, _ _:'Ss.J,c,._-½_1..,..--,,,Q=/e:d1cd2=c'.CC\>--<✓c__· ____ _ JRILLING LOG ) • ~DD?£S s 'c.._:-;±C-:e,(~· -d~,:___!.1~'1~):J.L.. __ ·.,Lz;'-P-.,--"'c.!'2:.<:../ c,(•Z::::::C,:/..:C' ,,....=· ~ 4. 70?W:).APHY: draw,v.illey ,slope,hilltop~irch: one) 5. USE 0? WELL: ~"1 ✓ DATE, 9-rO·-Jv . 'a 6. CO::S Ti-iIS h'ELL REPLJ.C£ AN EXISTING WELL? ___ /</ ____ _ 7. 707,\L DEPTH: 8. FO?.:-L;-:rrmi SA.M?LES COLLECTED: YES NO (_/ Depth Inside Wall thick. type Dia. or weight/ft. fro~ to ft ____ _ ~GROL."7: Depth Material l'iethod F:::o.--:i to ft --- DEPTH FRO-,,--TO D--I FOR..".ATIQ~; DESC?.IPTION o.!Z.J d '\Odd-!-&-~ a (J~ -~ ---\on--fe ~ Ir aca1.t1on.:i.l Spi:lC!: l.S needco, u5e ~ac,: o.:: ::o:::n 1-+:-SC?..E:S'.i: Dey th Dia. Type & Opening ft LOCATION SKETCH Fro.,1 ___ to {Shoe, Ci~t.1.ricc to numbered road~. or other :-. .1;i rc~c~crice ~o.!.ri:s) Depth Size Material Fror.i ___ to ___ ft ____ _ ' H. ST,WIC WATER LEVEL:-=-77.)fCl:t~lve~~; ;;,_ :;irins --~ GL. Casing is ft. above land snrfcce E-.:Lf::V: r33J t-,.-:-YIELD(gpm) : _____ HETHOD OF TESTrnG: ___ _ ~Pt.::-:?Il:G WATER LEVEL: ________ ft. -ru. 2 l. af.ter _____ hours at _______ gpr.i. ;,ir line Dcp-:.h ______ _ ccctify t:ru:: ::his .._-ell.,.-,~:, conc,truct.ed in ;,'..:;::0:-~.1::<:t..: •n·ith N.C. <1:1d ~;t;1n~:1rcls .1~c! th,1t t:i':i:: .._.i.!!l :-cconl i:.; true ,ind ~:-:,,ct.. ~!<;?~'.~Vu;,,, ,:(d{:{~;::,'.,,, ?-u::,c :: __ Jc ! I. . , I I Jg\ ::;::,__ ________ Date 9-/0 1.:::ac::.c::, 7m= c:e= JJ4a, ,-/:;J ~~ 1°~ 01 • __ ·1,,,_-::>_,_1~-_ft.; Dia.1'1 .. _i~/-/_in.; . • Ii-'! a Driller (k,d) /, b -<6d De.ta, Drilled :,,:-/V -!! o c::7 0 Cased to ___ ft.; Elev. ft. c.bova, HSL I .t~i.-=._ss. __ ~ ____ Elec. Log __________ Gar::.:::2. log ________ _ Thickness (Lset) I Description ,~~:~r:j (f~~t)I I /&-I// c,~, ,j_ "e-,J . / 7 _ DI~~ /4-J I . . . . . I I I · . / C ,, I.,__) dL SJ ,; .---~-----j------i-1------j-l ~~- I I I I .. I I I I I I ·-I I ~-~c t 6 ° I /i_ I f'So I {>:\.v,...,_ 0L_)J. ,;77, 7 I I .. . I I I l I I .. I L ( Gr-id Lo::.2.c::.o.'.1 (.__"' ;b 5~ !~u::b::;:-C.J Ju C 1._ ?. =-=-=-:-:-: 3 I I I I I I I I 1: --==--------,-----:-c---=:---------c:---------------------(? t=::q in g Tio=2., Air Tec:!perature,. etc.) ?:..:c._·_:'C: ::::sT ,OR CO:,STITUE,iTS OR PROPi::?.TIE:S _;_'.3 :;:;;n:cu:::::i. 2.:.·_-::-~:..·_,_::::3. S::'.CIIO'.), R."-1.EIGH 1-:.C. I ,,~y' .~ ~ I 1·=-- 1---· I Ca:-b~a Dioxide ....... ________ ng/l .?:.·.::i:-i=::::............. 2g/i -------- ::..s. :c :c:: e 3:; 2s ,:>.co3 .... ___ l}-_/o_O ___ c;/ l :==.:-:.=.2s.s, ::o= Ce:c~cn2te ..... ___ 4~.®-- __ ....................... u;;/l ---------~ = --. . . . . . . . . . . . . . . t..:.g/l -------- _::.:·~.::.-..:..=............... :.:~/1 -------- -~ ~; ~ ~ ~ 3 ~ ---......... ________ c~/l S~ecific Con~~~t2~ce (.:.,, c:-o::ihcs 2t 25°C) •. · rag/1 □z./1 ug/1 tg/1 r:.g/1 ------ ng/1 s :>cl i c::::! •............ ----..... -.. --------= cg/1 ng/l Z ic::c .•.•••• ----• -• -•• ------· ug/l rag/l T:'.'e,/ l -? .. ~c.=-~::i: L C .12 C C r L..._ r-L ,-- L i L_ C [ C [ I , __ _ ' I •--, I I I I I I I I I I I I I I I NOr'.TH Ct,ROLIN,1 01v1s:o~ c___, DE':ELOP,'-\i:~lT EN'✓I ~o.•:~::~n AL .--·.,\::.!,:;:::".::NT,. G?.Ou~:o·..-A TE R ., iCT IQ,",' P 0. BOX 27627 -?.;..LO::IG~!,. N.C. 27611 ;)_ -?...SG. ·:-;o. ' ·,.3:_1,. LOCr\TIO::: {Sho,.,. sketch of the loca.!:.io.i b~.!.o•..J} ~ea rest To·,..n : __ 72'-,__---'-'<Sc~cc·::-~:;;J;-,"'".-"'-'C'.'.'c:' _,_,,___,,-""'----~«~<'<--=<--= ____ Cou ,1 ty : ,--;/, ,;;-.,.., I:.: .. ~ ---<:ch-=,,l"--__ _,_(2""-_/"""---'-/~J~Se.aJ"--~-~--~-----Quac,an g l c No __ L __ ~_7.,_(s-=~'z'-------(:l.oad ,Co~uni ty or Su!:ldivision and Lot r:o.) 2. c-;.~:::::~: ,,1-t-·;£-7 '--[1 ~/,',.:'--C'"'______,, " __,:;,· SL-1--;,_,.f /}3 ~>, T,'<-LJ-e..,£ , .~ C . ~ , r;ro:-: TD ... ':0?CoJ~.APHY: dra.,,.,valley,slope,hilltop,_f_f8ci:-clc o~e) 5. ·,.::;::: O? WELL: __ :::::u_,.""-~%1:,...?C'a._ _____ Dl\TE :_~9_-__ /~(~)_-_j-v_' __ /' 5. ~0:::s 7a1s ~ELL REPLACE AN EXISTING w~LL? ___ ~P~-~~c)~- JRILLING LOG FO?J.L\TIO;l D:'..SCRIPTION cl, i c~odc!--~. RIG TYPE OR HETiiOO: ~ :; • ?J?.'-'~ .. ::ro:; SA,'l?LES COLL~CTED: YES ,;o __ ~=--------'--'/2_"-_,,"-''--i"-l_____.c,c.L"'-',0"-'-.c:;_/..c,e&o.';c,LJ.c( ·V'-L__;,(_7 ksc:,'uv,'.--'=-'-=--J-;::c:: a,,,.J Depth Inside Dia. to ft ____ _ Dept.h Mil tc:r i,11 Dep::h Dia. ?::-c:-: ___ to ft ___ _ Size ? =c~. ___ to ___ f t ____ _ Hall thic%. or weigh~/f t. Material type --,1 // above . h',\TER LEVELr</• ..;.ft.~C?f '\'" -a-· ;1g ---~~(__. is ___ ft. above land :.urfl:ce E.,:.:::-v: ..;...:;--:-YI::.~ (gp;n) :. ______ MET!!OD OF TESTING: ____ _ a:~e= _____ hours at _______ gpn. ~:-::..o?.!:-:ATIO:<: Typc _______ Arnount _____ _ :,;_.-_:-:::~ QUALITY :f_,~:~>:,?~-o,___/c,_/~C>"-''~'-n,::~rE.R.rYi'l.i?~ (0 ? J __ _ Inst<1llcd _________ _ /3 ~I / Ir acc1c1ona1 space 1s neecca, use bac~ oE ro=~ LOC,W!O:; S:i.E'I'CH (S:'.o·.· ciiSt,1:--.ci! to n:.:::.bc.rcd roads. a:-o:hcr ~.l\J rcfe:-cnce points) ) I ,33:J .2.:.;. •. ;:.:...:: T:f:=: o·.,:-:E:~ BEJ:~; PP.0\.'IOi:U T1 COPY o: Ti:!S P..E:CO?,J ;._:;; ::;:o::-.:-::::.o 0? TliE o::p;.__K.;:-s::-::.s REQUI:<2:-:.c:TS ;,:;() :-'~: :c.-~·-,:~::o;,: I O:J S? ,.::,,_, __ ,_,:, (.../ #-<//~-/0 , :.::i ;-.-;__.re~;,' c~=ti f:_: ::!\J.: l'.1i.c: 11,;lJ :-.:·,;·.:::.!":.ic:1c; LlnG Stan-:'..:i~.i:: iJ.!:CI Ul.'.ll / ,:,--~ ??I l,::.ic:, :o~::: ~·t:= :!.:-::. i:-": --·' :...-, c---_c~-~c-c-,•-,-:=-,-.. -,~,-,-,,-,-, .-c---_-----:--,--c-·o-.,-!;-,-,.-,-.,-,-,-0-,. -----th! 5 ~~11 re=~~~ i~ ::~0 a~~ J ___ //;.;' ,,--: I l,.,i.:n::> 1 ogic Log DEPAiff,·!EN'I OF ~:ATL'RAL A,\1) ;:co~:mac :R.ESOl?.C:::s r. GROl.Ji\'DWATER SECTrm; . I ._L~\g b}·: _________ Date 9-/D -ft-> Co.unty d,, j_G.?G-CJ Date Drilled Elev. f~. --c.bo'.,-2. 1-ISL ··t .. .;--s. _______ Elec .. Log __________ Gae:::.?.. log ________ _ I " --~5 I Description Deo·t:: (f 2ct) lfroc, I to I I £,d! ~il,,,-,, e(L ;., SC½d I r I /0'1 /ye-{ "' , ', ,, ~ ,+ ;'r ac,J I / 3 I'°'"' , I I I I Thickness (f2et) I I I I .--------.--t---, --;-,--- I I ·----------y--1'-.--- 1 I i ·-i ~-,___...,✓-,. {, t 0 s:::k<-> cJ'-/ f_. (;,.;rn // ,('--u I I I -------- / _, I L=ouna~ac~= ~ectio~ c;ou1.:y -4,./c / j__ Grid Loc:ac::.o,., L 6 / C.. -r....__-:-.·b -SE-~ t;u::i>ccr Cr-] f i) o 2.1 I I I I ?::::...:.:~ :-::::sr !O!\ CO~STITUE~ITS OR PROPE?.TIES .--\.S l.~ill~cx:~. 2::::.~:-:,:·_-_.: -:--::3. SECTIO~! ~ R.U.EIGH N. C. i..:.,:..a.lini cy (As CaC03 ) to pr: 8.3. .. . ... .. -<./ -c.g/l --------c 0 ;,Ci 4.5......... (,, Z G c:g/1 _.:..::.-..:::ir .. '..!.3.............. ug/ l -------- _.: _:: 5 2.::.ic. . . . . . . . • . . . . . ug / .i -------- \ . .~ -- C~;:-~onace ......•••••. ___ .L'._/ ____ ~g/1 C~=b~~ Dioxide ....... _· ________ □ g / 1 I! ,Y---: C::-,:'.::,;:-id,e .••••..••••• ·-~(o~'--t~· __ sg/1 ::-::.::.:o= (Total l:11') •• ______ /100:cl , __ 1- ·-- P~~2ol. ---·--....... . Soecific Con~~~ta~ce (~c;:-c=::10s 2. t 25°c) .. cg/1 ng/1 l.!.?,/1 r:.g/1 ~IL ------- ng/1 r::.g/1 ng/ I. Zi;::c: .•.•• --····,····· -------· ug/~ cg/1 v.g/1 L E: ~ C ~ .k::: ~ C .-- 1:::::: L -~ k: G:: E I I. I I I I I I I I I I I I I I I ',.,'::.L'.. RECO~D D ! VJ S IO,'t ( OF EJ\!'/IRON:~eHAL :-:..:.-,;..~~:•.::.Nr, G~our~o·,,ATf" '5ECTJO~ i P.O. BOX 27637 ?.ALEIGH, tLC. 276lll L [) ~ ,) c. 5'Ec. -;,:o. WELL CO~lST?.l!C?IO:• PS?..:H'i' }iO. 1. ;.;;:L:., LDC,\7IO~:: (Show sketch of the loc.1.tion b':!lo· .. ;) Q !-.'.cares:: To .... n: 7,_ .2_ Q (__,./ -f-(v\ \ l.-1\ ) rj ( County :_-1_/~~_..L/c.:'?L(,:_::_::;cc,,: _ _J""'"-'...-,;,_/c~X~·-------'.~~'-<✓-l-----'12..::?£=7~· ---'(_.,_)~-:>-"' ~>''---~~~-----Qu,,c.!r an<; 1 e No. __ L-=-'(""·.,,_7.,_<l""---'-/-'O:::_ __ (rtoad,'to;:\.".\Unity or Subdivision .ind Lot ?lo. l 2. o·,:::s,,_.L.(..!.::...il-J',~.rt--'-=---''---l-1i""-. ,_,,/~=:a;=o,<J ____ _ 3. '-'JD?-CSS' /Z; I (( 2.: 3 ,\ u T ,<.o~ DEPTII FRO:•: TO TO?W?..APnY: dr.iw,valley,slo?e,hilltO?,~i~cle o~e) . 5. L'S!: O?' h'SLL; --~?c=~~"'--"''9:,,/c....· ___ DATE: 6. DOES ?HIS hC:LL REPLACE AN EXISTING WELL? __ ~/\~/~C~)~- 7. 707.;i. DE?T:-1: ft D~p::h !. l. RIG TYPE OR V.ETHOO: ,q, i52• <' I nsicl e Dia. ---- Material Dia. n:s NO __ .ccL---'=--- W.111 thic%. or weic;ht/ft. type Type & Opening J~1LLING LOG FOi'L'~TION DESCRIPTION LOCNi'Io:; 5,.,:£:TC:'! (S~o·.· c!is:.:i?ice to nu::-.be:-cd rc.?.:!s, c:-o:l-.e':' r.:;;o.;, reference poi,,:s) Depth Size Material : r: o::i ___ to ___ f t ____ _ 1,. 3 ' ,, b S?A7IC r,·AT::.~ LEV.SL:~ ft.£ ~~~~i:,.-:::e4S::::.:.£.:.:_g ·--,s;_J Cb , __ Casir.; is ___ ft. above land ~urfcce LLEV: __ _ n-:-y I[LD (gpm) :. ______ MET!IOD or TE:STING : ____ _ --:-tr: PU:<.?1::G \,,',\IT.R LEVEL: ________ ft. ~ ;:,\S :-:::: o:-::::::P. n::::i:::: PROVIDF:D ?.l:C(::.·..:-·..::::o;..T 1 o:~s? ?D'.-'.0 0:S -~, _7,_ - ! '..:o ~~=~:l; c.:::-::.ify th.::::. thi:, ~,011 •h·uz: cor-::.:.'..·l:::";.1_•.C ~~, :1cco=Cc:·.c':! ·n·ith ;:.c. ·,-:!::11 Co:1::;:.:-•.:ct.io:1 ?'.~;;ul<!.::.io;is ,,~c! ~til~"..l~:-:!s .ind th.it this ·,1.:::1 r-:.:::::oa: is t.ruc <!:-:c! e:-<1-:::t. , .. ; Log '-~~ll ~io. :~/ Field ____ _ log :::,: _________ Date 9-// -Jzi Cou2.ty rb__L,,(/' /4/ / 3 ,? ] Z&r<kcZ'-,,,,_,..~,_,, /V :'... · Office ___ _ . USGS ____ _ I o:.c.::.c:r., ~m . .rn l"u :,::Sc~ m~ Jrja----0 <.-/ l=!''.::O 3 '? ' ft.; Diarn. Driller . I},, .. )~b ,,_,, De.cc: Drilled 9-// <" K Casesd .e ___ ft .. ; Elev. ft. c.bove HSL I/' .. G in.; I ..:::i.:::.g:s, ________ Elec. Log __________ Ga,.......:, log ________ _ I I Description Thic~ness (feet) ·--------'------i'-· --i-1-,--__ _ I I I I ·-----------;-----,1---,--,1 __ _ I I i I I I .. -1:rx,~ -I 11------------+-l--';l-+----- I I I I I I I / I \..OU:\Ly I I I I I I ?::.::.:.o: ::-::ST tO'-\ CO:iSTITUEcITS OR PRO?C:?.TIES .-\S :i3D:;:c;p_-;:'::!)_ ~--~·.--::-J·-·_,_:::3 SC:CTIO::, R.U.EIGH C:. C. I- I =X· ·--~ ·-- I 1$ 1:>< •- .=--.:..--=:..:Lr..~3............. ug/ l -------- / ....:-s::: :--.. i c.............. ug/i -------- :~!~rid~. --··········--~'-Q ____ cg/1 ::-2.::.:o= (To.:al MF).. /lGCc.l ------- ::-;,:;=r ........ : ...... · ug/1 -------- ··--0 ~~---a 0 c."°CO . 2__ '0 ~0 /1 ::..=._._ __ ::,., -· .. 3· ... ____ c ____ ~~ =~ :-~~~s~~r:Jon2te..... 4~ sg/ l ----~--- ---· · · · · · · · · · · · · - - - · · · u;;/1 -------- -~ -- - - · · · · · · · · · · · · - · t.:?,/i --------_._:.-.:..~.............. ~.s/l -------- :~-:-~~:lC:52............ t.:g/1 -------- :.=-:::·.::-~---........ - . - . . ________ t.:g/l '·-----'--' ..:··-=-";._· _:::.c• :-=-, .::•.:: 7 ::.?.c:· '=·..:\ "-a---"i.:.::s..:r:'---,- }ii::::-oge:1 ~j 2lC.2.i"..l .... -... __ i:..g/1 --------' ~it~ate & Xitrite. --------' ng/1 1!.g/1 tg/1 t:::;!,II Soecific Coni~cta~ce -0 (;:,ic;:o.:ohos 2.-.:: 25 C) .. ------- reg/1 r:.g/1 ng/l ug/l n-;;/1 r.z/1 L C 5: C C I L__.. ,- L .- L. C C C C C I I I I I I I I I I REFERENCE 11 I I I I I I I I I I I I I I I I I I I I I I I :1t POt;UJTA,NT,'CHARACTERISnCSi'· Ref. 11 ':orm Aoprovttd 0MB No. 158-R0175 EPA, 1.°'-NUMBEff": : If a· preprintm. label:~~ -~vkl<~ t1 it !in tha, designatedr·-&pllCIIS: RmMiu.. Info: '-,, ... ,, ~;.; etiotT canrfully;;:lt Bntp,_;af: la·'lst ;1,c:On~c:r -... -; through-·lti and.' entff.':.ttta:~_dara::;irr. ,-;..:: ··-:-:,.,-..... ~--appropriatr.-flll~n' anlla'·belO'IJr..fAlio;,:-lf.&Qy . ";·-$~ ·~4..;'~ ~ therpreprintiada'll►.l•absenfi:(~al'Mla:i; · ''·\. •.· i lofts oF thoi: lllbtdt sp,,oi;,llm:_th_.,lnltmntlt \. thoro·lliould>-/~-p1aaa,.·provlda.:l1,,;1n,; ,·propor-1111..,:;rr orea/r/: bel.,..,.;:,tff.ihei:lilbe: ·, compi.,.;imct. C0rl"llet.[yo,.; .-nao"""'!> ; ltamsX. Ii~ _IIJ.;~·:v;?:·ard.V.b'f11it:11,ii:t.'V/:elwtl :'musr:i,,,,·.camp1,,;,,di·~,Cbmplet1> ;" 1"'"'5:iFno-lllbal' ham:boeii-:proiridad::' Rafer •. the,, 1ruiructlor,.;.' !o,,-:demlla:l.i.-lteim: clOIC }'tioni:· and:". for-; thit l~;autfl(Q liatJi.:.l'ist:'.Wl ;,. "."hictr.thtidaar.:~ -~~~ec~?\~~'?~~~f-"~~"J{'. ~-INSTRUCTIONS:: eampieu' ~tliriiuglrr Jtu•dauiminswhlilbm:: yoll' 1181111:t1,'saibinit, 811\' pannit: application:forms to. the: EPk: If you~'.'vat !0.:9A\ ,.\'questinnf;:. you:miist ialmrit.thiscfo.mr;uml;tt,j;iupplam~.fnnn,I~ ill.'~ P.,m81Jthm:ir,_followinu;tha quastio"'-Marl<,':l<!t;iri th9'bai ii!:thal~mr. ;,;··if.th& supplamantlf fonn';.;itr,,cfjl!IE If, -~•ii~ ID mi:liiijulldiili: yin,.i nae<f nonubmit .• . '. ot1liaia.tiJims:'. Y.o..-.m,;y;IIIIIMl!C~iriif::ifj,miiiiiclMti l';uxciwhic1:ffi>i',,,paiu,ifriiiiuinline§_sal~ai>.C!nf.tiffi~~~~,1r,.t_.tha'i~•nst«itdefii1itio~i1,~~~ii.t~{ . · Is: t JS•.ar• 1ty-wh1 'f'c-resu.Jts. 1n ~•@;.:tlr.-••~•of.:the: u.s:..:othff;than_ thoss:describect. irr N,,.,..,::;-· ·:or :· ... .. M·2 .:·.:;':',~:~~:.:~,·r.;:--'.:-:~::_;:7::.':"'·i-:.~:..."'.".':· . Vl:FACILITY·LOCATION' s,.thsa,pra ,ty· ottJ-.·tha,r. OAt:· tNKJ·· :~'f:~i!t--·A or. 8.'M:IOflfl):wtric:t,-,·will: rew.1~~irr-:P:LI _ f --~,: _,,'·':.. : FORM2 ;; .. c·,-t-!'.'.·: ..,.,_:-..·,,:!:-~_f_:-~-,~.,,-~"'."~" :.:e: Oo:you..or.:will~yO&l.'.in;acr at"thll -facUltY' industriat-~--J.-.1\: mun~ effluenli balow,thadowwmol't"stratum ~7 ,:;,;; aanin;.,wlthhi·ons,:'~ mu~, of,.u-·-11: ~, "S, ·untJorvround:10Urcsof'drlnld~T (FORJ.\41):i;;;;'-'i i if.I Dci.voi.:oiwllfvailiinJoeiai:tli~!itciiltf.ftoliiifai,i,..'\ i~..:z.,.,_,ciD= Pi: ··11.1erua:mlning of:auffw: bvwtt'e.Frasd:lio~·: ~.-i ~ _, rnining,ot;.min.-ats:, im lltu:c:omi...;;; ~-:~~~-r=_~,~:~~i~~{RB'm\%7;;~1?.t4~~!-:~~ ,a· . _. :tPS · --·.22:r industriat:c:ateg0n.,.~11smnri:thilji~ : wlrich-will. poumtiaf 11(' omit;':ZSO: ttJiii,: air 'poilutanr.regu-undettbe:Cloani: ~ · · ln>a1.-aualim · · · · A·. STREE'T;· ROUTE NO. OR O:J"HER·SpECIFIC"IOENTIFIEff"!· .. ,. B. COUNTY NAME ,. . C. CITY OR"'TOWN O.STAT I':. ZIP CODE F. co_u I I e 'X ·~ I.xi /[ ;•~ i ,,., I j. I ONTINUEO FROM THE FRONT c;· Lv_,_"~s::;_1c~·co:...:.~o-ES..:..~/~4~'<i~•~·•~ir.~.~i-n~o~rdar:· ~-~---~•~o~:~P~'!;~:!:~::2:/~-~2;:::......:.....:.:::,;:;:.:;;;._;_.:;:J:.c.i::i""::::.f+~;...:;.::::;.ec.:r''i'~:.:;;~..c.'-"'·~:.,~-.:~·:_~-~..,~-~•~K::_::c~o~N::.::""::,:';:__..:....:....:....:...:.:.""-"-""-''-"-''--~-- l(specify) lfu:b:t==m_--,-~-~T-_HI-~~,,=:==~=~==~~~~==~~= I I · I~ th& facil it\l: · located-on: I ndiarr lands-l:"-' -~· l1i:c:.i:::....:. .... !':......:~::..:"'::.c""--''~·-2i~,..:.. ... ~~._::"--::,__.__~_. ___ ..,__ ........ = .... ,...-'~b-'=½.,+J,.J.i...:::q,c;::...::.,i,:;;;,;,;:,.,L~t§t~lg~-~-~_:_'.""_:i_·_,_rsf_p.;,·_;\~_~.-:_.~.-~.--·,:; ___ ._:_"_!_:-_t_;_t_'.~-]_:i_f_f"'_l __ .i_~_'.: __ ;_, . ~-& :~~' .~·\-' -~'~·:--.-,,.: ·•-,~-~ :_·: -f: ,,)~:::,'. ':·,~;-~·.<-: ;·; :-~-!-,,":~·,.;,::,:_ ~;".-.:3.f~-.-.r ,:.rt --,.~?~.,•.:,:,.:~,.1_::;~::::_7:~~~~~~%;·?:. ~--. :X:. EXl:ITI~ EN\11 RONMEN.TAI: PERM! I ; -~, :'.: '-J?t:ci{~t;;~-['°~';°"omLS~~"~~ ~.t.~}1_•:_t_~j?tJf,~\;¾1;~;~;[~i~tl~ ·~fj ._ ·16· 17 1a.' ••-,,--•-·• .· · · ~-· .-•• )0, • 1• H 17 • r - I ~~~~,-~~-•~t.U.~!i_t/~oA~i~;jtl ~"-~i1.-:~f"?~·:~:}~~:~~fspa:ifY.~-,,..:+:-_::.;.;!:-_.':~;~~~~!.~~;~~;;~~:~~;_::.~:{;: .-~~0~:-:.:~·-:;:;;;;_::;;_::,;;.~~~~1~~;~?,1:: $U~ ~~-~ l-=_,= •• +..!,:.~.~,.:.1-,-~--~ .. --,~----.. -,.-.~--... ~.---. ~ .• --~_-,_~. _-.~ .. -.-~.--.-;~-----~--=-~_;,;.~.~~c:i-c,.~r:,i,."~--.. -:.~---•. -.-•--.. -.. ~ .. -.. -,,~_-._,~,...----_--~--.. -. -._.-· ... -·_,--.~-~,d l.•~·:,_•:.::~~~~~~:-•:-:~.~~_/.J_~"-;:~~~~(~.Wan'~'f°;i;.~*:i:\~,'. ;!j./;J':,j_'/"";';_·;_-;.'.(1t~¥;-~-~~(Sp~f)r)/~•-:.'"'~-:O:~'-f:~~-;;.;{::·::~·:;.:.:~~-:'t·:~&/.';Y_:{i;:i_~-3.'.~-;.'.:•!;~j:C::·,f~~\;, -'• .. :.,~,;:;:\~,~-i:$:t~"i°;:,. 9" -R :<• . , ;x~MAP" .: . . -,... -. -. , I ~'An:a~fu; tlm(a-~iciii:i'on·:'?' n:,µog,_a/,lij<:rna~~thii,a_te,l·~~Ju,g'_t#t,!IIO.St'onuinTil"'beyond'p~o~ b_iiunde_ries;. The m_aj:;·tjltist:,ti01 ·•• : the: oistlirieiot'thetfacility;l_tr.e,_l(jcittioi,,_af-eac\t-of!itt'existii,g;andl~posedintalce, and:dischmgestructu,:es; each'.of'itshazardouswane,,, !. treatmiirii;.'· slaraiieitor''dispmallfucilitii!iiand\aach'i'welf. when!< it' injects. ffuidi undergrow,dLI nclude. alt springs;: rivers-amt othei surlaCUJ'"i-1 :x-===~~:!~=~~~precis,ifo,i:\i§,i1~11ts:;i/'.i:'f ; F :,''c~f:'°i?[•;:.,j;[!'i,,:; •·,, '.;, •· •••· •:·.\·.;:c·/:_!:•:'.'(.H~('~ .. · ~- , '-~ ;,.. 1'-J \, -. ~::, Q. <:', ,Xllll..CERTIFICA TION,(-irutructic,ns> ; /i:rirtify/und(!r penalty ot law thst:{' havrrpe;sm,sllyexamiried:and:anr.filinili~with the:information. ~bmitted in' this_'application and s/l :: s~'andi thsr;. based.' Oil' 117Yf inquiiyyof,· thOSB> per.;onsiimmediarefyc. responsibledor.: obtaining' tlie, information contained: i,r.th '. i,pplicatiarr,..'filieliuve that: the· infanmit:ion:'ii'tive{·BCCtJrnirand'camp/iJte;;. J/anr. awan,: thai::theni tire-significant:penalties:forsubmitti• ,:: fa/si,,.infonnation-;includinfithe-possibility, affine-and:im,imoriinent::.•::~:,.;; :'.--<-'· . . ·,-.... ;,,--... ... . . . . .. . . . . . '.. ._ ..... : ... ,.... . . .-•, .. . _ .... ·--· . .::. ·•. •,:;,,. A. NAME A-OFFICIAL TITLE (rypt! or prinr; B. SIGNATURE C. DATE SIGNED < , , I c.., f'"'r--, COMMENTs:FOR-OFFlCJAt:.:USEONCY EPA Form 3510-1 16-801 REVERSE I I I I I I I I I I I I I I Please prin1 or type in tne unsn<Jded areas only ·(f:'11-in ai·sas are spaced for elire type, i.e., 12 characrersfi[!.;C~h~l-;... ______ _,.--,-,,,------,--..,.,,..----- u.s. EN' NMENTAL PROTECTION AGENCY FORM 3· &EPA HAZARD01.._ WASTE PERMIT APPLICATION Can&olidamd Permiti Program RCRA (Thi, information is required under Section 3005 of RCRA_) FOR OFFICIAL USE ONLY DATE RECEIVED r mo. & d ,. .. II. FIRST OR REVISED·APPLICATION COMMENTS Place an "X" in the appropriate box in A or B below (mark one,box only) to indicate whether this is the first application you are submitting for your facility o revised application. If this is your-first application end you already know youi·facility's EPA I.D. Number, or if this is a revised application, enter.your. facility' EPA 1.0. Number in Item I above~ · A. FIRST APPLICATION (place cm-.''X" below.and providl_the appropriat• daU) .. ~ i. EXISTING F'ACILITY (See in,tructlon•·for definition of· .. ext.tlnt." facility. 71 .. . · Complete ltam below.) . n2.NEW· F"ACILITY (Complete item below.) ---;,.' FOR NEW: FACILIT1 ~=~~~=--,-,-,,-,,=-, PROV I 01!' THE" DA. T ,-;-;:--,r,--;:-:,:--,-,;;-;;-1FoR e:XISTING FACILITIES, PROVIDE THE OAT!! (yr .• mo., & day) (yr., _mo., &.day) OP.E T!ON BEGAN OR IS . EXPECTl!:O TO BEG OPERATION BEGAN-OR THE DATE CONSTRUCTION COMMENCED, (iu• the bo.:ce, to tht1 left) N (placa an "X" beJow and complete Item I aboL1e) D 1. PACIL.ITY HAS INTERIM STATUS~- " III: PROCESSES -CODES AND DESIGN CAPACmES 02. FACILITY HAS".A,RCRA"P~RMrr"• ,, A.. PROCESS cooe-·.;,;,;. Enter the code-from th&·lirt-of process.codes below th.et best describes each· process to be-used-et the-facility. Ten lines-ara-providecHo entering codes. If more·lines-era·needed, enter the code(&)-in the space provided~ If-a process will·be-.usechhet is no't·inciuded.•in·the: list-of-codes below,jth£ describe the-process lincludingitsdaign_c11p11ci'ty)·in the-~ce·provided.on the,forrn lltem·l/1-CJ. · · ·· · · R,;.. PROCESS.DESIGN-CAPACITY/-FGr' eactJ.coctw8nt8ract irr coh.im·n A-enter th& C8pacitv.caf the-process-.... f. AMOUNT-Enterthe,amounL. . .. .. . . . . ,. . · -·•-. _ . . . . . . _ _ . , . __ .. 2.." UNIT OF MEASURE· -ForB&Ch--"amountentered:in·oolwnn 8(1 }-, enter the-cod& from' the list:of unit measure codes below that' describes-;tha un~ofl"-' - rneesure used;: Only-the-units.at measunrthat·are.-listedbetow,shouJd·be-usect.· · .. ;,,/:·:·--.,.: -i-:J · PRa:/.' APPROPRlATEUNITS.OF· . PRO.:;,: APPROPRIATEUNITS.QF CESS, .,. MEASURE FOR PROCESS"" . :;c_cEss;::; MEASUREFOR·PROCESS, CODE -OESIGN·CAPACJIY PROCESS_'· rn ~CODE r.,··. PfSIG/\' ct311.i;;rIY · PROCESS: Stonge: CONTAINER (ban-el,.drum,.etc.L · S01-·; GALLCJN9' OR" LITER5"- TANK. soz"'. C:--ALLONS-OR·LITS:RS~' WASTE Pl~· .·. 903~\ ~=:~~~~~Sc:~· SURFAce:1MPOUNDMEN-~-- Disposal: INJECTION WEI.:.~. LAND Fl LJ.. __ .L.ANO'APPLIC-ATIONt•. · OCEAN°DISPOSAL SURfPACE. IMPOUNDMEN"n': .-.. ,· ·-·.-·... . . <(- UNlrOF MEASURE'". SCM,.;, ,' GA&.;.LQNS,OR: u:-r~s-:c ;_ z:::rni:•.~-G"ALLONS: OR' LITE'RS oao,·:~-ACRE-Fe:~ (the uohune.that.~ •·::.c· would:couer one acre to.a.,._-:. ·.·.depth·oton• foat) ORi-. HECTARE-M~ER• Ost· . ACRl!:S',OR·HEC.TARES·· oaz:. •, GALLONS PER"DAY OR: LITERS-PER CAY 083a;. ~AL~':'~OR-UTERS,.~. UNITOF. MEASURE: CODE·. ·. UNITOF MEASURE' T...unent: ·_,., .. ' ;;,':; ·_"':i · ·. · .'. •-_:_:\~/-:~:~,::::.'-.' TAN~--c-:-·-~·: . c~TOt_: ··-~oNS P~Y-·-oR~··•: ·.-,:__:·,-.-UTERS.PER"OAY.".·-·.· ;·: . SUAfPACE IMPOUNDMEJtri1:--: TO.Z" ,-a~.t.ONS PER-Q,AY-OA".·.~-- INCJNl!:RATOA: -:. _c·:. T03~ ~-~~::.~g~ o~/•,.'.. ·.- _·.t.:, ·---. . ·. '-ME°tA'JC:TONS-PER.HOUR: . L.~-· ··. -.:G°At:1o.ONS Pl!R1'f'OUR''0R'! -.. ·: . CiaTENS PER-HOUR .. · :. .. : ~THER'(U1e forph-y•ica£.Chernu:aJ;-.,.~--. To~ ::;c:o::J ONS"PE~.y:Q~•/.:·. thennaJ or·biolol(ictu treatment .. --:-:--· . ~TERS.PEA,DAY,;'.·:: :.;_;·;:.", . ·=::~:n';»':,~=~~~~i~::;._ ,.....~ .-·<-· :_ .. ·, · .. ·. : N:;?{.f·{:: a tors. Dacrlbc the proceau in ,:,. . • ':" ·. ,. ... __ .. : . the •POL:e pror;id.ed; Item lll-C.) -,--:. ~--· . UNITOF MEASURE" CODE UNIT OF MEASURE GAi-LONS.. .... : .. : .• : -• C.-LJT!!:RS-Pt!:R-.DAY:-. ~-.".: • V .· 'ACRE-FEET:. ... _; .. ~--~. A: :-LITERS . · .. ::.· .. : .; ;_: ._ •. ..:·. ·:.: ·: L::·;-··.-,,~(_.';,· .. TONS,PER° HOUR~ •.• -: • .• D; Ht!:CTARE-METER;, __ ;_· •. _·,:~::_-·. F CUBIC YARDS..... • -_.:·~·-• v<::,::: • · METRIC'"TONB;Pl!R"HOUR;. .... _ •. • w,'.· ·. ACRES~·;· •• · .·,... -·-·./; .• ·:,}-'. S CUBIC M~ERS-. ~-• .• ~. •. ~ -•··•••-•. C.:.:_: ---~~~-/_.;_,:.:;:_.<.ALLONS.PER,HOU~;.,~ .•.• :,. ··; ..• _.~; • E".·~· . HECTARES:; .. ::, . ."-~:-·•··;·., •. ~ .•.••.• :..:.;:·. Q. GALLONS,PER DAY."·~ .:. ;_ •.• · ... u:.~---~-··· _ -:-', L:.ITERS-PER HOUR-•, ••• • •.••• _ •• •• H·.:~·-. . .•.. , _ , . .-· _ EXAMPLE FOR COMPLEnNG" ITEM' IIJ: fshown· in li~nwnben·X-t-~. snd.X-2"/,elow);. A-facility. h8S;two storege-_·tanlts;. one.tanlc·cen·hold.200·gae1om and:th, ,other can-hold·4(Xlgallons:,.. The·.facility·also·hm,andncinenn:o-r:that.CSn-·burn_ up.to 20:gsllons:per-hour; ;· · _:·-'·. --:~,-~~-=i."'.; __ ;\•:'.-<.'.:.·:'• __ .. -·_ ., ·. - · ... -_. •.--·-,:::-.. : B. PROCESS'DESIGN c:A.PAc:ITY .. ~ A. PRO.!---------------~---. FOR' ti.I~ g~~ z .. uNrT· OFFICIAL Z:,~ (,_,__m li,t 1. AMOUNT 0:UMR~A-. USE. ,,v (,pecif-y} . ONLY .J-z above) (enter--code) u .. X-1 S O 2 a:: A. PRO:..,_ __ s_._P_R_o_c_E_ss __ • o_ES __ 1G_N_,_c_A_P_A_c_t~T_v __ .... ~ CESS ti.1::; CODE ·z-::, (from,li,t J z above) L AMOUNT ; ,. ..,,_ 5 .. •.. X-' TO 3 20 E 6 7 I 2 8 I 4 " 111 U I 9 h. 10 " ,. " " ,. If " r:011 C:--.,.,. .. ,., .-, ,~ ,,,.., Continued from the front . . PROCESSES (continued) • SPACE FOR ADDITIONAL PROCESS COL. OR F"OR DESCRIBING OTHER PROCESSES (cod, :04"). F"OR EACH PROCESS ENTERED HFRE INCl.UDE DESIGN CAPAClTY, A.. EPA HA . N M ter the four 1g1t number ram R.. ubpart D or each listed hazardous waste you wd handle:. I you . handle hazardous-wa,nes. which are not listed" in 40 CFR"; Subpart·D, enter. th&four--digit.numbur(.sJ: from 40 CFR~ Subpart C that.describes. the,chera~; ... I tics and/or the toxic contaminants of thOIS hazardous~ · : · 1 • , • ' • • • · · : _ • ESTIMA TEC7 ANNUAL QUANTITY -For each 11:stad wasc.-entered in column .A eat:JTT18Ut"-~e-quantftv ~f ~ waste that ~ill be• handled on 'an aO:,uat basis~. For eaclr characteristic or toxic contaminant entered in column A estimate the total annual quantity, of all-the non-Hsted waste($) that will.be'handled-' . which posse,s;that characteristic Or com:aminant.: -. • · . . .. ". . . . • · •. . . . . __ · . i I I ~~ a~ M~RE;~ Fo~ .. ch q~i~ ~nteredln col~~"-B e~e, the unrt of rneaw~code. Un IS, of m991Ure wh;clTm~ ~~~ and th&aP~f ~~ . I ENG[ ISH-UNITOF·MFASUBE CQQE".: MFTRICUNITQFMEASl/RE' ...... , .. · ... · cooe· I.,·.;.;·,.: .POUNOS'.,, •.•.••• ··•-•···-• .:. • ••• · ••.• P-· KILOGRAMS-••.•.••.••.••.• ~ ...... ;· •• ,, ••.• .-.,, _ _-K. '. TON~.".·~.·;..:· • .-: . .-••.• ··---· •.•• ·., .••..• ·----•• :· ..••• T', Mlt.1".'RIC.TONS? .. .'." ......... h••·· .: •.••.•..• :-•• ::_.:-• .-~"; •• M~. ... . . . . ·,.. . . ~-' If facility· records-usa,any othef"unit" ot·meelU18',for quantity~ the,units. of measure must be converted:into one o'fthe required:unitt.of. measure tuldng,into.:. · . '. account the appropriate density or-specific grav_ity. of the-~·-~. · ·· · · · I PROCESSES-: . 1; PROCESS CODES: . . . · · . · . . . . For·Uasd, hazwdoua:wasta:-For each Urtad.-.ha:zardous•wasta: entered ·in•column A selectthe-code(sJ:from,the-list of process:codes.containecHn· Item IJ f :: to indicate how the waste will be stored, treated, and/or disposed of at the facility. · I. · For non-fisted hazardoua·wastes:: For each· characteristic. or·toxic.contaminant entered-in column A, select the-code(s): from· the· lisr of process-cod .-contained in. Item· Ill to. indicue·alJ.the-processes. that"will be-used to.store, treat"~ and/or·dispose1of all'the-non-listed· hazardou.-:W81t:8S:. thar--posu -: ·. that characteristic or toxic contaminant. . · . ' · · . · · · Note:. Four spaces· are-provided for· entering· procesr--coder:;· If mora·are-needed:-(1): Entet-.the·first three es.described:above; (2) Enter "OOO~in·th&.• extreme. right box. of. Item I V-0(1 l; and. (3) Enter in the spac:a provided .on· page-4; the line. number and .the additional code(&). · ·• P~OCESS DESCRIPTION: If a code;. npt listed for •·process thet.wlll be used, de=ibe th• p,;;.,.;.. In the space prov;ded on,the fomi. . II : NOTE:. HAZARDOUS WASTES DESCRIBED BY MORE THAN ONE EP.Ac HAZARDOUS WASTE NUMBER;·_ Hezardounvams thet can· be· descri-by-.-.-nore than one EPA Hazardous Wasta Number shall be described on the form as.follows:. l: 1 l Select f th EPA H rdo WBS19 N be d ante ·t · ol A O th e rne ccm late column B C and D by estimating the total anne I . one o • aza us um rs en " 1n C umn n e·sam · 1 p • . quantity. of the·waste and describing BU the proce-sses to be used to treat, store, and/or dispose of the waste.~ In column A of ·the next-line:enter the other·EPA Hazardous Waste Number·that"can be·used·to:describe-the:wast&.: ln.-column·D(2) on-thet·fine enter-"included with above~• and.make no·other entries on that line;. 3. Aepeet·stap 2 for each other EPA Hazardous Waste.Number that CSJ'l be used to describe the haz:ardow.weste. lr:PLE FOR COMPLETING· JTEM' IV (shown in-fins numben X-1; X-2,' X-3; and X-1 below)·-A facility will treat end dispose of an estimated 900 poun ·. year of chrome shavings from· leather tanning and finishing operation. In addition, the facility will treat and dispose of three non-listed wastes. Two wastes I 1re corrosive only and there will be an estimated 200. pounds per year·of each waste; The other·W'8ste'-is·corrosiw and.ignitable ~nd thefe-will be en estimated ' 100 pounds peryear of that waste. Treetment will be-,n arf"incmerator and disposal will be in a landfill. l A. EPA c. UNIT o .. PROCESSES: _I HAZARD.. B. ESTIMATED ANNUAL OF MEA· ~ WASTE NO QUANTITY OF WASTE. f~~e; t. PROCESS COO ES 2. PROCESS'DESCRIPTION J z. (enter code) codei (enter) (lf a code 16 not entered in D( 1 ))· -it I I I I I I I I \ K 0 5 4 900 p T 0 3 D 8 0 --I I .. ' I I I I ' ' ' ' .. 7 X-2 D 0 0 2 400 p T 0 3 D 8 0 i j ....J ' ' ' ' ' ' ' ' D 0 0 1 JOO p T 0 3 D 8 0 - I I ' ' ' I ' ' IJD a o 2 included with above ! orm 3510-3 (6·801 PAGE2fJF5 CONTINUE ON PAGE C I ... Coot;nueo from page 2. -, -I NOTE· Photocopy this page before complating if you I, ,ore than 26 wastes to list I I I I I I I I I I I I I 1· I I I I I Form Approved 0MB No 158-S80004-•,,-.-------------------.-..-EPAI-D.NUMBER(entirrfp-omptl/lrJJ .. ,~· •\"\ ·.,,._··.~··· l"OR:OP'~Cl.'AL..UBlt"ONL.Y' .. . _. ._.,. --~-·::: . -:···\ wk.:ldLlb~lz..1.:sts1517111zi"'i1 \·· ,~\lwl •. · ·.···. DUP m DUP . ·. · .... ·• .. • .• I I • UIUII& flt • Ul4UJJ • ta :V. DESCRIPTION OF HAZARDOUS.WASTES fconttnued! A.EPA . c.. UNIT 0; PROCESSES::· . "' z· _o .JZ I 2 3 4 5 6 7 8 11. 12 13 15 .'16 'l7. 18 · 19 20 21 22 23 24 25 HAZARD. B:-ESTIMATED ANNUAL WASTE NO. QUANTITY. OF WASTE-: (enter code} l>lx (' I/_ U 1 •1 " EPA Form 3510-3 16-80) OP' Ml!:A• _ SURE ,. (enter· .· ·-. -·-; .. r:..PROCESS.CODltSt. .. co"K· (enter}.· ... _ • . . " ' .. . .... _ ··, ~ PROCl!:SS DltSCRIPTTON'··· · (if a codtt ia·not entered-ln,D( l)F .. :•: ::.; :-·- .. •,~ · I I I I 11 Ir (i" ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' 1.", I I ' ' ' ' + . ' ' ' ' I ' ' ' ' ' I ' I ' ' ' ' ' I ' ' ' ' ' I ' I ' ' ' ' ' •. •' I ' I I I .. I I I I ' ' ' ' ' ' ' ' ' ' ' ' ' I I I I I I I I I I I ' I I I I ' ' ' ' ' ' I I I ' I ' ' ' ' ' I ' ' ' ' ' ' ' ' I ' I I I I I I I I I I I I I Z7•z•Z7•nz7 z•21•1• CONTINUE ON REVER IV. DESCRIPTION OF HAZARDOUS W. 'ES (connnued) E. USE THIS SPACE TO LJST ADDITIC.. .L PROCESS CODES FROM All•existing facilitias:must include in the·space provided on page 5 a scale drawing of the facility (see instructions far more derail). V[PHOTOGRAPHS Alf existing facilities:must include photographs·(aerial or ground-level) that. clearly delineate-all existing structures; existing storage •. treatment and disposal· areas; and sites of future storage, treatment or disposal areas· (see instructions for more derail}. VIL FACILITY GEOGRAPHIC LOCATION vm .. FACILITY OWNER f8l'A. lf:the facility.owner is also the facility operator as listed.in Section VIII on Form 1·, "Generat Information", place an "X" in the box to the left and . skip to Section IX below; a::. If the,facility owner is not the facility operator as listed in Section VIII on. Form 1', complete the following items: 1. NAME.OF FACILITY'S"L.EGAL OWNER• z. PHONE NO. (area code & no.) H'E'u r Le L_j r. lu-12 7/ 3 4. CITY OR TOWN- ' I certify under penahy of law that I have personally examined.and am familiar with the information submitted in this and all attached. ocuments; and that based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that·the· submitted information is true, accurate, and complete. I am aware that there are significant penalties for submitting false informatiorr, . including the possibility of fine and imprisonment. · A. NAME (print or type/ B. SIGNATU~ C, OATE SIGNED Ji < =---· ) C /',-~1' }'.j / / • OPERAl'OR CERTIFICATION cenify under penalty of law that I have personally examined and am familiar with the infonTlation submitted in this and all attached documents, and that based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the ubmitted information is. true, accurate; and complete: I am aware that there are·significanr:penalties for submitting false information, ncluding the possibility of fine and imprisonment. A. NAME (Pnnt or type) B. SIGNATURE C. DATE SIGNED I . ' I -:(. PAGE 4 OF 5 CONTINUE ON PAl:Jc. I I I I I ' I ' I I. I I I V. FACILITY DRAWING (see page4/ ~ ~ iJ.. L6M ; l , l \st-~ /,2 Lon} f ~i--~~--, -----, ",,~~· ---=1~/~l}~L_b_n_,~___, i• ~i~------~ I ~ ,. to I 'I .~- F I I· I 1 ..,,,.~,..., ,,-.. nnl oFFTCe .J, □ Form Approved 0MB No. 158-$80004 I I I I I I I I I I REFERENCE 12 .. I I I I ii I I I I •·.: .. ,. .. I I> I RETURN TO: PAULINE ANDERSON U. S. Environmental Protection Consolidated Permits Branch 345 Courtland Street, N.E . Atlanta, Georgia 30365 0 0 Q I O 2 Agen~l C:: !VE D EP1\/REG!Ot1 IV JuL E E'r'"'''\''.•,: u.c \I VI_•;_,.,._, SECTION 6@@7 S,:6z;{ QUESTIONNAIRE Ref. 12 SU.8 1. I have reexamined the definitions £or treating, storing or disposing of Hazardous Waste and I wish to withdraw Part A of the permit application. Yes •-----· No ---- I 2. I have reexamined the definitions for treating, storing, or disposing of Hazardous Waste and I wish to add the TSD activity to my original Notification. Yes No -------- •Yo¥ I AAf-ll c/{!,~t.E, I ; .. '. I I I I I I I I I I I I I I I I I ., I 1 --:'~.~- ,. :.:, -· UNITED STAT:C:S Ei--JVIRONM[NTAL PROTECTION .c\GENCY JUN 5 f9Bf 4E-CP CERTIFIED MAIL RETURN RECEIPT REQUESTED REGION IV 3.15 COURTLAND STREET ATLANTA, GEORGIA 30308 i,CD0ti255:, 79 ~ fl· .4. _,q. f ~~r f r1s~ ~, .a-nc., .::1s:·ct SLr-l..1.--.li.i,., ...,c .. ,lcb SIGMON MARY bOGKh~EPER RT 1 'i !JO;; 3~0 STATESVILLE: ·-------· Re: Section 3007, Resource Conservation and Recovery Act (RCRA) Request for Information Dear Notifier: Our records indicate you filed a notification of Hazardous Waste activity pursuant to Section 3010 of the Resource Conservation and Recovery Act (RCRA), 42 U .S.C. §6930. That notification did not indicate that you either own or operate a facility .engaged in the treatment, storage and/or disposal of Hazardous Waste. However, our records show our having received Part A of the applicatioil for a permit to operate or continue to operate your facility. Pursuant to Section 3007 of RCRA, 42 U.S.C. §6927, you are hereby requested to complete and send to this Agens:y the attached questionnaire in_ order that we may determine whether your application submission was proper. I£ we have not received the completed questionnaire from you within ten (10) wo~king days 0£ receipt hereof, you may be subject to appropriate enforcement action. If you have any questions regarding this letter, please contact Pauline Anderson of my staff at 404/881-3446. Sincerely yours, H,?i-- A_cting Direct~v . Enforcement Division Enclosure (1) cc: State Director I I I I I I I I I REFERENCE 13 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I o'l. o'l. ·o'l. Cnte~pzi°JeJ, !Inc. Slgnon Septic '7anlt & 7'oot ec,mpaHfj Route 14 · BOX 350 · STATESVILLE, NORTH CAROLINA 28677. (704) 873-8954 April 19, 1982 Bill Myer Department of Human Resources Division of Health Services :'. 0. Box 2091 Raleigh, N. C. 27602 Dear Mr. Myer: 1 O April 13, 1982, A. A. A. Enterprises, Inc. received a letter from the Division· of Health Services stating , our Facility I.D. No. NCDo62555792 has been deleted as a generator and transporter, We do not want to be re-moved as a transporter. Respectfully 3wmnited, 1 MLS/rs Ref. i3 I I I I I I I I I REFERENCE 14 I I I I I I I I I I - -- -- - - -- -- --" ';O~TY =~ ,,, .... . OUAO NO.,_~•~-~· ~:~~ .. __,1-"f.-.s1::r:i ,\L MO. ~,l~~~'~?~·~'~'~--'J3 LOIH.J. lo: ,\fiO, FRO, r/1,WO·;, r-:~~0. 'Ncf30, WiRO. ·-.. -· -"S-'-A"-l•cc,I '--P-=L-=E~.:..P_._R.:.:_lc i R I T Y \\'0HO, l<ins1on F() Snipr,ecJ by: Rus, DATE F!ELD Al✓ALYSES L1\BOflATORY Al✓f\LYSES 8005 "0 mg// COD Hi\lh 3'0 mg/I coo low :ns F.!Q/1 Colitorrn:Mr t !!cal 3 l 6 16 / 1 00ml Coli!o,m:Mf Tota I 3 1504 I 100ml ~--•/ ,, TOG '8D mg/I lur!Jidlly '/t:, rnu ,.;_" '" 4 QJ uni rs .-\1"-aliniir !O nH '' 5 "0 mg/I Al~.:, lioi Ly la uH ll.:l 4 If, rnQ/1 C ~ rllur><! 1<• 4 4 ~ 11111/I Bic.irtJon.ile ,, 4 0 mg /I ' Arsonic:Total 1002 -~-'' ·; ug/1 ,, ca,bun dio <Ide ,os mg/I \\ ✓. )(" Chloride 9'0 mg/I Chromlllrn:Ho, \032 uo /I Color;Trul' 80 Pt-Co C1anidu 720 moll □ HOUl INE CJ ;,,1ERcrncY Owner Loca1ion or site PUFlF•_iS[:: B,'\SEUi<JI~, COl.\f"'L,\11-!T, C()!.ff'L.1.<1,JC:f. !....US~ I cir 1; IC 01111.l '' Description u1 :;;J1np!inq point S;:irnpl i nq l·Je tliod Rem;:irks (puinp';' baiter, etc· _·_-c•1-c-"' "'~"""'+"'"·'c-ic'-~·:c-1-;,..._ __-cc,o· '"'c1c· --si~-;c·-------------------------------------- S~mpl,? llll(;IV(li (pumping lime, air terno, eic.) Diss. Sot ids 70300 mg/I r,,, AO Sih·er 1077 -u,;;/!. ''' c' -) ,· .. Organocrilo1ine p,.,s1icid6s --fluOrido 95' mg/I H a1dness: Tota r ,00 mo/I ' ,( A< Aluminum 1 1 OS J .-1,) I''() 1· i uo /I t!-' , ,, ' s, • Barium ·1001 I I ,·,· , ug/1 Oroanopt1os;111urus f'esticidas , .. -Hardness {non-carb) '°' moll -·· Ca Calcium 9 '6 r.1 ) mg/I --~-·--: Acid Her(licid~S Ptieno/s 32730 ,.-, uo/1 -,• -X. Cd Cadmium 1027 < /t) u,;,/1 Sµocilic Cond. 95 uMhos/cm 2 ;/._· Chromium:Total 1034 i::;·,-. ~ ug/1 )· Gase/ Neu1ral E,1ractabla Oroanics Sul r ;i tu !)4 5 ' i mull·--,;<: c, Copper 1042 S?"J· ug/1 Acid E~lr,lcl,,tJlo Oroan,cs Sul tide 7'5 mg/I :--; ,, Iron 1045 ;;"7/',/l(\ ug/1 - ;-( Hg Mercury 7 >900 (t) ·, ug/1 Purgea:ile Or,;,anics {VOA botlle) " K Po1assiurn 937 ,..., . I ,...,,,_/_ nHJ/1 / Mg r,lagnesium '" ' :)(· mQ/1 •..,/ 1.2 -l)ibromocthani, (10013) tJH3 as N 6' 0 rng/1 TKN as ,, 625 mg/I r-:.~ Mn· /.1anoem,su IOSS // f1r)(·)ug/l '" Sc><.l•urn !.)~!) / ,~--;'./ rng/1 N; N, ck e I 1 06 7 -~ ' -~-(() ug/1 Pb Lead 1 05 I .. :'JI -:~) ug/1 tJ02.,. N03 as t1 630 .. ,; mo/I ··,. ;, ,/ s, Selenium 1 1 4 7 ..... ,:.:' ,., ug II P:T o!al " p 665 mg/I ,' '" Zinc 1091 i/./ Jr) U',J/1- ' .,;~ ·7~ ' I,,' ,. ·a · ;' L n b Com rn C n Is: ,'c'c·c· -~c· •c··~e--~,",~""~'"""-=-;..,=,","' :,:c'c·a•'+,·--•c'_.c<c•'~~-"""-,c''•,,-.~-~c'·-c,_' _c / V ✓--"(' .-i . .,,.; ,,, -~✓~--_J ... -1/ ,..., / for Dissolved An2.ly:;i:; -st:i·,:,-;il tillcru: s;;r.ople <!nd write ·01s· in blud; Wt1ite ·copy -1-lcodqcrnrter:, Pink cc;;y -Region• YeJ!ow copy -Lab i I I I I I I I I I I I I I I I •• I :0...;purte.J oy , ,.,_) Checked by 8J.C.- Superviso~ Lab No. Sample Type ;, v---/--;;1 tG--\~r,\ 'T',,~ ,Aod·,·,,-j o, 'no-_\~r1,~9A ORGANIC ANAJ.-YSIS Entered Checked Analvtical 01 n 0-o , -v-n .A J /4n,_-tri ,·Qrf , , " , ·.JJ o ,,-t-, a .i n ,,.Q _,rn ~ In ,On(¾ :vo .,1 -' Results O, , , G C / t=Pv.'.) " ~~n O,' A r:.c / r-r V /1,-1 roZ_,.,-1, fo m ... , -. , f'·,.,. r-1.n~o ,t-n ... 0 Q' \ - V V r::_,_ '"" o o /io,,n r(\.-,-~ffi_,'1.Q_ rr,Q,,4,...,~0 rn n , ; -Y OJYt n.,, A,, 0, Jlo r,'\ r,u, n, I r /; 0\otor➔o,1 0\..-v\ (✓ / MS: a V 'Y7u-. n rs .... Q • _]-.nnl~·,,' ...Inn r-1 ~ n r--V---n ,O ~ r--c/F.c ~ ~ t /icu! "1 . ,·· J A..:" !-;"~'} .. /,,.~?Fr.1,,t,,(·1 JI;.,,;~, J_.7:.~-,'.<f/t~ ----. . . ,/ I ( r s,-,L,,:,'}~~-p6y L_ ./ /_,, -;.;:/~,,_,_,,..( ,_.,.,._ 'r .1\7,,., •. _. / , i,, {J ,,_._,;_ ,'.,• . ~- , ,, .::.::-<.~-\.{! / ,:,,;;,_/· ,. , .., -·e ..,...::..)_,,.> /' r:,i ~/.,,.: .,,_-t"I ~--.: ~~/ :. _., ' !--__ .l:..::J_/..,, 7; -~ I ,:, ✓·-~ .:~:----t/-: ---,_;, ·,, --~ .,T.,A --,-,' , __ L_ C/HS/DS •Jsed Concentr.J.tion ,.· ' - -------·:u ' . N.CLJPARTMENT Ol & COMMUNITY SAMPLE D ROUTINE. PRIOR IT)' r1 ,_.,.,,· L.:".( EMERGEt,JCY DATA DATE DATE R7o c,,;,_,; TIME PU8POSE: BASElll·JE, CQl.1PLA1t.JT, (circle · moorw: omi;t FIELD ANALYSES pH400 /~42-D Spec. .lb a TP.mp. lO -~~-C Appearance ,,-!ft._.,/j..,. I JI,-.,,.- Cond. 94-~ at Odor . A/t;l7 'G- . ' Owner c.. ,. v Lo ca! i on or s i te _,.,,;·_. • .O,c' _,_J .J/c::.:,., <.;,.._...c_ ______ L..:.Ll.<.,..'-.::-:tf:=_· .c~-l."'---------.,--'------------- Description at sampling point (. e . i ; Taste jJ/)'? ,,-. /) r: i e Id Alia l y s i s 8 y: --~7_··_·_._~Y,~•-~--~~~t.._,_~_~ _____ _ Sam pl i nq rvle th od --,'~)~r,~,~·:c":I ~'-"··~···ccc.::-:----c:-:ccs------.,-----.,-Sam p! e In IC r ,, a I --~~·.,.L.~7~·----------- ,--·j (pump, bailer, etc·.) Remarks ~2-i,' , .... ~ ... f ,.,<.(._ 3 Lf,?.-7 LABORATORY Al-JAL YSES HOU5 3 10 rnu/1 COO High ''° -mg /I COD Low 335 mg/I Coll!orm:MF Fecal 3 16 16 1100ml Colilorm:MF T olal 3 \ 504 1100ml TOG 680 mg/l T url.>1 d I (y 7 6 /HU pl{ 4 03 uni IS Alkalinily 10 pH '. 5 '10 mg/l Alkalinity ,o oH B. 3 ' " mg /I Carbona111 "5 mQ/1 Bicarlwno.te "' mg/I y Arseroic:To1al 1002 -< ,:7n ug/l Carbon dioxide 405 mg/I X Chloride o-io ;;q mg/J Chromium:Hox 1032 uo/1 Color:True 80 Pl-Co Cyanide 120 mg/I Lab Cornmen1s: GW-ti•1 1-luvi:;r;d 7/B5 (pumping time, air temp, etc.) Ul,;s. Soll ds /0:JUU mu/t X Ao -!illvur I 07 I -c:::,-;; ~·_) uo/1 Fluoride 951 --rng/l :x' Al -Alumin·um 1 '°' /.;:l .nnO uctl Ha1dness:Total 900 mo/I .x -,, -Barium ·1001 J,,...::;o UQ/1 Hardness {non-cart,) 902 mo/I 1 c· X c, Calcium 910 qq mg/I y Phenols 32730 .--· ·\ uo/1 /. Cd Cadmium 1027 < /,'). U(J/1 Spec!{ic Cond. 95 uMhos/cm2 --:'.• y Ch1omi um:To1al 1034 <_le; UQ/1 ;,( Sul I ate '" C/ mo/!· -~:., ·x c, CODD81 \04 2 17 ug/1 Sult Ide 7'5 mg/I >( Fa -·Iron 1045 (JJ () () ug/1 >< Ho· r.1 ercury 7 1900 . ·1~.:i. ug/1 x· K Potassium 937 c;, ;-me/I -,( 1,10 1.1aoneslum 927 /--:?.,_ m,;;./1 y Mn·-Marlganel'ie 1055 ?r.;oo ug/1 J( Na Sodium 929 . -:77 mg/I NH3 " " 610 , !(.; mg/l X tli tlic ke 1 1067 < 1";() UQ/1 TKN " N 625 mu/I / Po Lead \ 05 1 ,< ~n ug /I X N02 -t N03 as N GOO // , ;,l, ll)g/1 X So Selen;um \ 1 4 7 <,:JO ug /I P:To1a1 ,sp 565 mg /I X z, Zinc \091 <I.::. uc/1 For Dissolved Analy!>is -sui)mit fill>'i·rJcJ saniµle and write "DIS. in block While copy Headquarters Pinh ,:opy -Region Yellow copy -Lab I ll r<J,inuc hlur I no !'us1lcld0~ y >( Organoohosphorus poslic!des .. / Acid Hordicides X: Base I /-Jou tr a I Extractable Organics / AC; d Extractable Organics y PurQeablo Orcanics (VOA bollle) x~ . 1. 2 -Oinromoelhane (EDB) y {,<.,,,,?-; .. ~/ 1 r--. x' ~/,~,.,..,.,.-. / ,, I .:.J"'. ,. I . s~ ' '< I)-, . ••v,ql ,''lfF,., v/S .o U,?,.-, ,,,.,O.o iv1c~ 1. Reported by Date ,-,.!_/o!.0/,;,:, ,. ·--"--;,l-"--,7'--"'--"----:-.\~,.' ~\ Alt\ 1 Checked by t]_I--'-' ORGANIC ANALYSIS '·'{ .. ·-.Supervisor<]?f:K Entered I I I I_ I I I I I I I I I I L,ib No. -/(T-\':l,os ---·------- -- ,- ; ' -· ; r· i I .. ·- Checked Sample Type : kl n:ft-o • Analytical Results Tu--J..n..-.~ :t-~ ';_ l •,...1 ~r.-. rl. rr1 • , ·ffo ..J 0 '--' c:,c / r-\Db ' V rn,-,rnr-V-, ~ ,·,\Or 1',-\n'"-ti~ ,·o,-1) '=' JI n,, r\on,L I inrl ,~n ~O, ~ --l V V ,-.,n -• :1:, 0,, r.:.clc::., ' V I I rl ,·, h V rn ,-,.irf (/.,n,. 0 ,\" 4-n, hi,\ 0 \ , (:.r;,L20 +,' n'r J , ,n ; ,I o ~ -J;: i f, n ~1 J,Q/1 f1 fun Ao~o,'i-o ,l V . 0 ' -Ge /':.l,., O 0 -V "Y\,-,.. 'l~n-:h-Jo K.n~M\rr A oi o -vci-r1 0.Uv. ' " (:,r / /JI I[) ---I .){,n , , ~, ,I orvrl:,·,; o-1 J,on .... On,., ,,Q oio ,'to ,i Ou. (:.Cl M,· V ' · C~,n~-9n.:ri, ~-o,:h : •. ~0 o _, QA.. 'J {) Jvi-:l I ;.,_ );-" 0... /1.AA1T1 • M i'""--f on n• • 0 n I}-" ,., A !. o A. I ! ~ , ,j 0'V< 7 i 1 A O ,Y ~l - " .. , ,Q o ~-Js, 'o · n Ji # ')_ V I I 'i "\r ~+, ,U .() .n ~ -~ V . I \ 1Y< 1 rf/ o "-t; i ' ; n ,0 4f l/ 1,-'• An,,.,7',ti:•or) µ ~) V , J "· ,' cl n ro-/, 1 'J , n A ,t!-C V r-(';"." (Or1.J. 9;011Qr(.r '~lea 01 oi. O -To r.l Q )..)J, Cc/EC. I GC/HS/IJS •.wed • .. I Concentration o -:::. '"' ,..,,c,/ e ' I i ' •. I l"l.v.."'!e 11:: ',_,,_/(? i2_,_.,,1 e \\ µ.;--,/(' \ r( _c..,i (' ! I 'l, ,,,.,r, IP ! ' -... -C<JUM f'r l--r-~ .... -1 OUAO NO; /~ ~:f:_ / :r I_,; T. - - I I SEGI A.L h!O. T-~ Ill!' !i6 75" -·N.c(.)l'ARTMENT OF - - .. & COMMUNITY Dl'\tELOPMENT Hep_ort to; ARO, FRO(~~-~~?~) RRO, WaRO. WiRO,. DEM GROUNl)WATER FIF! i"J/L,\ll FORM SAMPLE Pfii'.)RITY \\/SRO, i-::ins!o11 FO 0 ther ________ _ □ ShirJPCd by: Sus,(_~-~;:~~~ Ott1er _______ _ COLLECTOR(S): -7·-,{ -:i---~ DATE ()J C'i .Z.<i FIELD ANALYSES Owner cJ AOUTI NE [1 __,/ [i,l[AGEHCY PUF1POSE: 81\.SELIME. COl,1PLAli,JT, (circle pl1 400 -~--Snee. Cond.g,; L oc a Ii on or ::; i I c _cc~·--"''~--'-' L.:;~ -0,~-------------~-0~• :...:-~1~'.J"--"-~=---=4=-·-~"------------------- ,, Temp. 10 ~,~,-~ __ 0 c ' Odor -·~•~•-·0~>~•~·-"----Oescripti~n of sampling poin1 .,. ! I Appeurance )Jj-._)J,_, Taste -~--~·~/--'-_/~_:.:.l=·--;, ---~-,":J I• Cir../._./ Samplinri Mel11od .. .,__ (purnp7 h~i!er, etc.) Field Analysis By:-~/~-~'~'~--~-~-'~'•~--------Rc111<1rks ~·-~•;=•-c'--=~-'-!_-c'·tr:=--'{'I~ ·-_.7 ..... ,,, (purnpinq lime, nir temp, etc.) LABORATORY Al-JAL YSES E:lOD5 31 0 mg/I COD HiQh :HO mg/I COD Cow 3 35 mg/I Colllorm:Mf Fecal 3\G16 / 1 OOrnl Coli1orm:MF Total 31504 1100ml roe 680 mg/1 Turbidity 76 !HU PH.~03 uni ls Alkalinity ,o "' '-5 <>O mg/I Alkallnily ,o oH 8, 3 '15 molt C11roona te ~ ,\ 5 mg/f BlcarUonate ''° mg/I · Arsenic:Total 1 00 2 ug/1 Carbon dioxide ,05 mg/I Chloride '" mo/! Chromivm:Hox 1032 V\l/1 Color:True 80 Pl·Co Cyonldo 120 mg/I ,,v C-·,' ·-' //•.-,<.l.. Lab .Comments: "· ' / ., <· I . cw-5,1 .Revised 7/85 DI ss. Solids 70300 mo/I A.,;i Silver 1077 ugl1 Al A.1.umi-n;m .. Fluoride 951-· molt I 1105 UQ/1 H ardnoss: Total 900 mg/t "" Barium ·1001 ug/1 Hardness {non-carb) 902 mo/I 1,+·· Ca Calcium "6 mg/I Ph,lnots 32730 · UQ/1 Co Cadmium 1027 UQ/1 Specific Cond. 95 u/.1hos/cm2 ~-;',:.· C hrom!uri1: Total 1034 uo/1 Sulfa le 9'5 mg/I".· ~~r~-.. -c, Coooor 1012 . ug/1 SulfhJe 1" rrig/1 Fe Iron 1045 ug /I HO Mercury 7 I 900 ug/1 K Polasslum 931 mg/I ~-1 0 Magnesium 927. mo/I Mn -Manganese 1055 ug/1 '" Sodium 929 mg/I . NH3 as " GI o mg/I Ni Mi Ck c I 1067 ug/1 TKN as " 625 mg/I " Lead 1 05 1 ug/1 ' NO2 -t NO3 as N 630 mg/I s, Selenium 1 1 4 7 vg /I P:T o taJ as p G6S mg/! '" Z Inc 1092 U\j/1 '' -r--.) ( ,/ ' ,/ li .(~; !I ,,/,' _.(' ' ,' -4--~-: -..<.L ., ,,· _,, ,_,:,· t.'' ·<",. ,·, _,,, ,' ... , ,:' ,. " l/,, ./,l.✓ ..A V •· ,, . ·-. //"' ,' --~ " V Par Dissolved Analysi::. :;utlmil tiltG:-r!d ci.irno!e and write/_~01s· in block White copy -Headquarters Pink copy -Region Yellbw copy Lab Organ_ochlorine Pes1icides - Organoohosohorus Pos1icldos A.C, d Ho1dic;dos Base I Neuual Extraclable O111anics Ac Id E11rac(able Organics X Purgoable Or11anics (VOA bollle) ,--d n / - ''' Oit>romoethane (EOB l / . I I /./i".'f _;) I-' -~-~ ---~ / -,I /_ /__,,.I ---- - srn, AL No:T-R W /, '7l neporl to: ARO, FRO, f:~~) RAO, \.VaRO. WiRO,· 1NSRO, Kinston FO Shi.pped by: Bus,(~Q(J~;r\ COLLECTOR(SJ:T ,,_(C,7/ f'IELD ANALYSES Other ______ _ DATE SAMPLE D .ROUTINE Tl r,; I': PF:IORITY r;./ u.J·· Elv\EF!GEr-!CY ·:-;:: < ... , 13/\Sl::.urH.:;: .COl·,lr"LAIJ-rl, ;., ::; :.; (<;:Xrcle _.. I c·. tj ··•.~~ C Q7;-.-i PL I /1 I! r, 1-; o"n/J)· · pH 4 00 c;-; 'J lsoec. Cond. 94 (·, S .... a 1 2s0 c Owner :'):~_,_.,.,,-:: S~...-:'8-::-:c -rr:,~,L~ J'),.-,1),#'~ ... Loe a ti on 0~1 site =5'~--'~'c~' __ ,LI I·:;--~: ________ ,_·.,_-'-?~,··_,_,,c;.~l~ • ..L-#.-"-·~\-~;:_i,.~=j_:: ____________________ _ LABORATORY ANALYSES BOD:, 3 ,0 mg/I coo High 3'0 ---mg/I coo Low 335 mg/I Colirorm:MF Fecal 3 1616 1100ml Cot!1orm:1,IF Tota I 3\504 1100ml I •oc r,ao mg/I :urbldl ly 7G /HlJ PH.403 uni ts Alkalinl 1\' tu i,H 4, S "" mg/I Alkalinlty 10 pH ,_, "5 mg/I Carbona lo "' rtlg/1 Bicarbonate HO mg/J )( Arstinlc:To1al 1002 --:: r) ug/1 Ca,bon dlo~ide 405 mg/I X Chloride 9~0 . ,. mg/I Chromium:Hex 1032 ug /I Color:True 80 P1·Co Cyanide 720 mg/I Lab Commenls: G\V-5,1 Revise:d 7/85 De script ion ol su rnp I i n~J poi n 1 -~cl ~/-~/~!_,c..c~.l{.},__ ______________________________ _ Samp!inq /•.1clhod Remarks J (pumping tirne. air temp, etc.) Diss. Solids 70300 mg/I ix Ag -Silver 1077 -< "J.:.--:::-ug/1 Fluoride --mg/! 95' x' Al -Aluminum 1105 /....,.:? l!l)d ug/1 Ha rtlness:T 01a I 900 mg/I I ,· I ,,-· Be -Barium ·1001. 4.,1 A() ug/1 Hardness (non·carb) D02 mg/I '>(' Ca -Calcium 915 }JC? . mg/1 ,.I' .Phenols 32730 .,.--· ug/1 --, x Cd -Cadmium 1 0 2 7 < / /") ug/1 Spi,cl I le Cond. 05 uMho~/cm1 .,l;-'" Chromium:Total 1034 7',< uo/1 )< Sulls 1e 045 ~ mo11" I )( Cu -Connor.1042 ~;,:.). uv/1 ·-Sutrido "5 mg/I I ;.) Fe • Iron 1045 Jf;:; "" 0 ug/1 ' >c Hg Mercury 71900 / /J.,:-J ug/1 y K • Potassium 937 1rr rnQ/1 >< I.IQ -Magnoslum 927 :JI moll 56 x Mn -l.langanese 1 055 vdoo ug/1 : V '" -Sodium 929 §1~ I mg/I -, NH3 as N 6'0 /f? mg/I ~~-ni flick el l 06 7 < ,-,() ug/1 -· TKN as N 625 mg/I "(' Pb lead 1 05 1 I 'l r, UQ/1 X N02 1' N03 as /J f.30 /} -,r mg/I i v' s, Selonium 1 l 4 7 --<:JO ug/l P:T 01al as P 665 ; mo/I I Zo Zinc 1091 I 7/) U',l/1 ! I ' I ' For Dissolved Analysis -suG.-1~il fil!Gi'~i,1 i;ample and wlite ·01s· in block White copy -Hcadqu.irters Pink r,r.py -Region Yellow copy -Lab }<-o,ganochlo,ine Pesticides -. -- ;.( Or',lanophosphorus Pesticides y Acid Hordicides ><' Ela so I No u tr Rl l:, trnc 1abl e _Organics V AC Id £xtrBCIOblo OrQan!c, y Purgeablo Organics (VOA botlle) " '. 2 Oibromoettiano (EOBJ V .-? r-. -.• ..,. ,_ -,(' _,.-,,} .. , . X Y'. I. I . ' ,E ATTACHED ORGANICS ANALYSIS REPORT -. - ·- I i I I I I _I I I I I I I I I •• I- I Reported by--'(-"-':::::_-Date r;2//(,/ft I I ·~,~ \ Checked by fn_C__ ORGANIC :Supervisor~ K Entered bY..._1..:;:_,c..._ Checked ·b~ Lab No, Sample Tvoe ; I, 1, .f-.... Analvtical Results ' 7r_ -1"3.oY '11-,An~'1,·.:~o~ r4oTn, fr, -~ 0, ' <'~ C / F'.\" \0 ' V . l'(\k •,;o-l:-, .',Jo. /..lo_, t ,/\ ,·nA , n.J ' .I , " ·~ ~ o -!~ 0; n ' D, ~. GJ:..l;c -, V V ·--().,_ rkrriJ~,v" o .'Y\,, n 0 -.h ·On 1'17 ,.., ,,_ 'p,.,._ ,.() 0 {J-0 r VD j D, l A 0 ., r , J ri._l -0 0 ' Of\• n , , .. ; I n,. i-·1 ; ; n _0 •-r -0~ rlinhi,+n..!) o~. \) 'T V r..c I'"" \o I !)1,, 0-An {Y\ 0' .+,., ~ () ,-r, r.,,·..11 rJN 6'1 ,"I •-(/ n (),.f () ,-'I\ 'l - - • ' . --..-l rrto ,&r, J1 n, "' , r:., /n, C 0 IY\,.,. A,,· _/I .\hnnO,.;'.,:.Oo, ,..!ln-OorTO-~ n, .. ('✓ IF.C . ' I ! I ( '• / \, ( Concentration ' ' I. ·I I I I I I I I I I I I I I I I State of North Carolina Department of Environment, Health, and Natural Resources Mooresville Regional Office Jam~ C. Maron, Governor William W Cobey, Jr., S<:crccary CERTIFIED MAIL RETURN RECEIPT REQUESTED Albert F. Hilton, Rq,~onal Manag,:r DIVISION OF ENVIRONMENTAL MANAGEMENT August 9, 1990 Mr. Henry Sigmon, Jr. Sigmon Septic Tank Service Route 14, Box 350 Statesville, North Carolina 28677 RE: Dear Mr. Sigmon: Notice of Violation 15A NCAC 2L Classifications and Water Quality Standards Applicable to the Groundwaters Sigmon Septi.c Tank Incident No. 3422 Iredell County, N.C. Chapter 143, North Carolina General Statutes, authorizes and directs the Environmental Management Commission of the Department of Environment, Health, and Natural Resources to protect and preserve the water and air resources of the State. The Division of Environmental Management has the delegated authority to enforce adopted pollution control rules. Based upon an inspection of your facilities located on Route 14, Box 350, Statesville, North Carolina, the Division has reason to believe that you are responsible for activities resulting in noncompliance with North Carolina law. Staff of the Mooresville Regional Office (MRO) of the Division sampled two monitor wells at the subject site on June 14, 1990 and the lab results indicated that the North Carolina groundwater standards have been exceeded. Specific violations-of 15A NCAC 2L .0103(d) -No person shall conduct or cause to be conducted any activity which causes the concentration of any substance to exceed that specified in 15A NCAC 2L .0202 -are as follows: 919 Nor.:h ~in SrlT't"I, M=rnvillc, N.C.,:28115 • Tc\q,hon, ?'CH---663·16'19 • FA.X ~653-60-«J I. I I I I I, I I I I I I I I I I I Mr. Henry Sigmon August 9, 1990 Page Two Concentrations of Substances Found in Exceedance of 2L Standards on June 14, 1990 (in micrograms per liter, uo/1) -Constituent MW-3 MW-4 2L Standard Iron 590 2300 300 Lead 86 1 9 0 50 -Manganese 430 50 ··· Mercury 6.0 < 0 . 2 1 . 1 1 , 1 Dichloroethane 1 . 3 ND ND (ND -not detectable; --means not analyzed for) You are responsible for causing, contributing or allowing the continuing violation of the underground water quality standards because you are storing septic tank waste in unlined lagoons. To achieve compliance with the above-cited laws or regulations, you are required to submit within sixty (60) days from receipt of this letter a site assessment report as prescribed in the ·enclosed outline. As a part of the site assessment, two monitor wells should be installed in the vicinity of the state monitor wells that were accidentally damaged. This data will then be used to submit a remedial action plan which will be due within sixty (6Di days after the site assessment report is submitted and approved by this Office. The above violation of 15A NCAC 2L is subject to a civil penalty assessment under the authority of G.W. 143-215.6 of not more than $10,000.00. Failure to respond within the time specified and to voluntarily achieve compliance may result in a recommendation for enforcement, the issuance of a special order against you under the authority of G.W. 143-215.2, or a request to the Attorney General to institute an action for injunctive relief. Your response and/or questions should be directed to Chris DeRoller of the Mooresville Regional Office at (704) 663-1699. Sincerely, Brenda J. Smith, P.G. Regional Supervisor cc: Office of General Counsel ?erry Nelson Enclosures: CMD/pl Site Assessment;Guidelines Sample Results I ' I I ANALYTICAL TESTING t. CONSUL TING SERVICES P.O. BOX 31486 4 CHARLOTTE. NC 2S2:l1 • TELEPHONE (7o.4) 527~183 • FAX: f70,,I) 525-().400 March 7, 1991 AAA Enterprises Attn:Bar·t·y Sigmon Rt. 14, Box 350 Statesville, NC 28677 Dea•· AAA Enterprises: , ./ ?:_) I I I I I I I I I I· Below are res1~lts of analysis of 2 samples received fat' examination onFebr1.1ary21, 1991: Cust o ■er Code: AAAENTER Pho"Je N,.1~ber: <701t) 873-8954 LAB I. D. AA04173 Bold ID r,,_,mber G910Fl-2 Collection Date: 02/19/91 S1.1bmittal Date: 02/21/gl Customer Sample l.D#: MW! ~'-ibmittal Time: 17:46 TEST i:•ARAMETER UNITS M1.1lt icomp □nent analysis: ACID EXTRACTABLES I I 4-NITRDPHENOL PENTACHLDROPHENDL 4,6-DINITRO-D-CRESDL 2,4-DINITROPHENDL 4-CHLOR0-3-METHYPHENOL 2,4,6-TRICHLOROPHENOL 2,4-DICHLDRDPHENDL 2,4-DIMETHYLPHENDL PHENOL 2-NITRDPHENDL 2-CHLOR □i:•HENDL '-'9 /I ug/1 ug/1 ug/: ug/1 ug 1/ 1 I.\ g / j ug/1 ug/1 '.19 / I' ug/1 ·. Multicomponent analysis: BASE-NEUTRALS I. N-NITRDSODIMETHYLAMINE ug/L BIS(2-CHLOROETHYLIETHER ug/~ N-NITRDSO-DI-N-PROPYLAMINE ug/L NITROBENZENE ug/1:. 1 I· HEXACHLDROBUTAD I ENE '-'9 /L 1,2,4-TRICHLORDBENZENE ug/L \ rsoi:•HDRONE ug/L I NAPHTHAJ_.ENE u g / L BIS(2-CHLOROETHOXYIMETHANE '-'g/L ~~~:;~~~~,~~.~2~.~:·;:~,:;R k~~,tr-c,c, ~r-,. ,';'~ I);-, BY BY GCMS Not Not Not Not Not Not Not Not Not Not Not GCMS Not Not Not Not Not Not Not Not t~ 0 t i~ •J t TEST RESULT Det Det Det Det Det Det Det Det Det Det Det Det Det Det Det Det Det Det Det Det n p t-. DC:TECTlON LIMIT 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 1 QI 10 10 H:l I I ANALYTICAL TESTING&. CONSUL TING SERVICES I I I I I I I I I I I I I P.O. BOX 31486. CHARLOTTE., NC 28231 • TE.l....EPH()NE (704) SZi'-4183 • FAX: [704) 525--0400 RRR Enterprises Page: 2 March 7, 1'391 BASE-NEUTRALS BY GCMS (continued) ACENAPHTHYLENE ACENAPHTHENE DIMETHYL PHTHALATE 2,&-D!NITROTOLUENE FLUORENE 4-CHLORDPHENYL PHENYL ETHER 2,4-0!NITROTOLUENE DIETHYL PHTHALATE N-NITROSODIPHENYLRMJNE 1,2-DIPHENYL HYDRAZINE HEXACHLOROBENZENE 4-BROMOPHENYL PHENYL ETHER PHENANTHRENE RNTHRRCENE DI-N-BUTYL-PHTHALATE FLLJOR/'.1NTHENC :-'YRENC: BENiiDINE BUTYL BENZYL PHTHRLATE BIS(2-ETHYLHEXYI_I PHTHALRTE BENZO (al ANTHRRCENE CHRYSENE 3,3'-DICHLOROBENZ!DINE D1-N-OCTRL PHTHRLATE BENZO (bl FLUDRRNTHENE BENZ □ (kl FLUORRNTHENE BENZ □ Cal PYRENE INDENO Cl,2,3-cdl PYRENE DIP-ENZ Ca, h) ANTHRRCENE BENZO Cg,h, il PERYLENE 2-METHYLNRPHTHRLENE B!S(2-CHLDRO!SODROPYll ETHER 4-CHLOROPHENYL PHENYL ETHER HEXRCHLDROETHANE ug/L ug/L ug/L ug/L , ug/L ·ug/L ,ug/L ug/L ug/L ug/L ug/L •ug/L '-'9 /L •Jg/L 1.lQ /!.. ug/L l.tg/L ug/L •.19/L ,jg/L tig/L •Jg/L u·g /L •_tg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Not Det Not Det Not Det Not Det Not· Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det I Multicomponent BENZENE CHLOROBENZENE analysis: AROMATIC VOLATILE ORGANICS 1· I 1,2-DICHLDRDBENZENE 1,3-DICHLDRDBENZENE 1,4-DICHLOROBENZENE ETHYL BENZENE TOLUENE XYLENE METHYL-TERT-BUTYL ISOPROPYL ETHER ETHER ug/L ug/L ug/L ug/L 1_1g~L ug/L ug/L ug/L ug/L ug/L Not Det r,ot Det Not Det Not Det 3 4 2 b Not Det Not Det 1121 1121 1121 10 1121 1 0 1 0 10 10 1 0 1 0 1 0 10 1 0 1 0 10 1 0 10 10 10 1 0 llZl 1 0 10 10 10 10 10 i0 1 IZl 10 10 10 10 1 1 1 1 1 1 1 I· ., I I ANAL YTfCAl TESTING & CONSUL TING SEFMCES I P.O. 80X 31486. CHARLOTTE. NC 28231 • TEl.EPH()NE (704) 5.27--4183 • FAX (704) 525--0409 I I I I I I I I I I· ARA Enterprises Page: 3 March 7, 1991 HALOGENATED VOLR·rrLE ORGANICS BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON TETRACHLORIDE CHLOROBENZENE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE DIBROMOCHLOROMETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,}-DICHLOROETHANE 1,2-DICHLOROETHANE 1, 1-D I CHLO ROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE CIS-1,3-DICHLORO~'ROPENE TRANS-1,3-DICHLOROPROPENE METHYLENE CHLORIDE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE 1, 1, I-TRICHLOROETHANE 1, 1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE VINYL CHLORIDE CHLOROETHANE I·. CIS-1,2-DICHLOROETHENE ETHYLENE BROMIDE LEAD, TOTAL I I RON, TOTAL MERCURY, TOTAL MANGANESE, TOTAL (cont i n1.,1ed) 1.19/L ug/L ug/L ug/L ug/L ug / l_ ug/L ug/L ug/L ug/L ug/L 1,Jg/L ug/L 1~g/L LJQ/~ ug/L ug/L ug/L ,_,_g/L ug/L ug/L ug/L •og/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug'/L mg/L mg/L mg/L mg~L Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det rfot Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det e,, e,3e, 20. e,e, IZ'l.002 15.QlQl 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 I 1 1 1 1 1 1 1 1 1 1 1 1 1 e,, ei2e, 0. 0·2 e,. e,e,2 ·IZl.02 I ------------------------------------------------------------------------ Comments: · Samples collected at MW 1 at sludge pool ·_ .-VAL:KCR I I I I I I I I I I I I I I .;, I' 1· I I ANALYTICAL TESTI_NG & CONSUL TING SEAVK:ES P.O. BOX 31486 • CHARLOTTE NC 28231' • TaEPHONE (704) 5.27--4163 • FAX· (704) 52:5--0400 AAA Enterprises Page: 4 March 7, 1991 Custo ■er Code: ARAENTER Phone Number: (704) 873-8954 LAB r.o. RA04174 Bold ID Number G'l!0F1-2 Collection Date: 02/21/91 Submittal Date: 02/21/91 Customer Sample I.D#: MW2 Submittal Time: 17:46 TEST Pi=<RAMETER ,LJN I TS TEST RESULT DETECTION LIMIT ---------------------------------' -------------------------------------- M•.<l t icomponent analysis: ACID EXTRACTABLES BY GCMS 4-N I TROe'HF.:NOL ug/1 Not Det 10 PENTACHLDROPHENOL ug11 Not Det 10 4,G-DINITR0-0-CRESDL '-,' g / l Not Det 10 2,~-DINITROPHENOL ug/1 Not Det 10 4-CHLOR0-3-METHYPHENOL J.(_g / ~ Not Det 10 2,4,6-TRICHLOR □e'HENOL ug/1 Not Det 10 2,4~DICHLOROPHENOL ug/1 Not Det 10 2,4-DIMETHYL~•HENOL ug/1 Not Det 10 PHENOL ug/1 tfot Det 10 2-NITROPHENOL ug /1 Not Det 10 2-CHLOROPHcNOL '-' g / l Not Det 10 Multicom~onent analysis: BRSE-NEUT~ALS BY GCMS N-NITROSODIMETHYLAMINE ug/L Not Det 10 BlS(2-CHLORDETHYLl~THER ug/L Not Det 10 N-NITROSO-DI-N-PROPYLAMINE ugi/L Not Det 10 NITRDBENZENE ug1/L Not Det 1121 HEXACHLOROBUTADIENE ug/L Not Det Hl 1,2,4-TRICHLOROBENZENE ug(L Not Det 10 ISDPHORONE ug/L Not Det 10 NAPHTHALENE ug/L Not Det 10 BISl2-CHLOROETHDXYlMETHANE ug/L Not Det 10 HEXACHLOROCYCLDPENTADIENE ug/L Not Det 10 2-CHLORONAPHTHALENE ug/L Not Det 10 ACENAPHTHYLENE ug/L Not Det -10 ACENAPHTHENE ug/L Not Det 1 0 DIMETHYL PHTHALATE ,_,g/L Not Det 10 2,6-DINITROTOLUENE ug/L Not Det 10 FLUORENE ug/L Not Det 1 0 4-CHLOROPHENYL PHENYL ETHER ug/L Not Det 10 2,4-DINITROTOLUENE •.1g /L. Not Det 10 DIETHYL PHTHALATE ug/L Not Det I 0 ~-NITRDSODIPHENYLAMINE ug/L Not Det 10 · ·1, 2-D I PHENYL HYDRAZINE ug/L Not Det 10 HEXACHLOROBENZENE ug/L Not Det 10 4-BROMOPHENYL PHENYL ETHER ,.19/L: Not Det 10 PHC:NANTl'.JRENE ug/L Not Det 1 0 ' 4<9 SPRli✓GBROOV. RO!>Jl • ('.1-i/J.PI ni-r-c ,,1r ,-,r,.-, • .., I I I I I I I I I I I I ANALYTICAL TESTING &. CONSUL TING SERv>CES ' P.O. BOX 31466 • CHARLOTTE, NC 28231 • TTlEPHONE (704) 527-tlBJ. FAX: (704) 5.25--0,400 AAA Enterprises Page: 5 March 7, 1991 BASE-NEUTRALS BY GCMS ANTHRACENE DI-N-BUTYL-PHTHALATE FLUORANTHENE PYRENE (continued): ug/L ug/L ug/L ug/L BENZI DINE BUTYL BENZYL PHTHALATE BISC2-ETHYLHEXYLl PHTHALATE BENZ □ Cal ANTHRACENE CHRYSENE 3,3'-DICHLOROBENZIDJNE DI-N-OCTAL PHTHALATE BENZ □ (b) FLUORANTHENE BENZ □ (k) FLUORANTHENE BENZ □ (al ~'YRENE lNDENO (1,2,3-cd) PYRENE DI BENZ ( a, h) ANTHRACENE BENZ □ (g, h, i l PERYLENE 2-METHYLNAPHTHALENE BISl2-CHLOROISOPROPYL) ETHER 4-CHLOROPHENYL PHENYL ETHER HEXACHLOROETHANE ug/L ug/L 'Ug/L ir ug/L ug/L ug/L 'ug/L 1ug/L ug/L ug/L ,.19/L ug/L ,:,g /L '-' g / L ,.,g/L u,g/L ,ig/L ' Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not D et Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Multicomponent analysis: AROMATIC VOLATILE ORGANICS BENZENE CHLOROBENZENE 1,2-DICHLOROBENZENE 1,3-DJCHLOROBENZENE 1,4-DlCHLOROBENZENE ETHYL BENZENE TOLUENE XYLENE METHYL-TERT-BUTYL ETHER ISOPROPYL ETHER Multicomponent analysis: BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON TETRACHLORIDE CHLOROBENZENE 2-CHLOROETHYLVINYL ETHER CHLOROFORM :HLOROMETHANE DIBROMOCHLOROMETHPNE 1,2-DlCHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE ug/L ug/L ug/L ug/L ug/L ,.,g,/L ug'/L ug/L ug/L ug/L Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det HALOGENATED VOLATILE ORGANICS ug/L ug/L ug/,,L ug/L _ ug/L ug/L ug/L ,.19/l ug/L ,.,g /L ug/L ug/L Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 1 1 1 1 1 1 1 1 1 1 1 1 I ANALYTICAL TES?ING & CONSUL TING SERYK:ES I I I I I I I I I I P.O. BOX 31486 •CHARLOTTE.NC Z8231 • TB_E?H()NE (7D4J 577....C 183 • F.AY.:. (704) 52>-0,400 AAA Enterprises Page: 6 March 7, 1991 HALOGENATED VOLATILE ORGANICS DICHLORODIFLUOROMETHANE ( c □ n t i n 1.1 e d ) I 1, 1-DICHLOROETHANE 1,2-DICHLDRDETHANE 1, 1-DICHLDRDETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE METHVLENE CHLORIDE 1,1,2,2-TETRACHLDROETHANE TErRACHLORDETHENE 1, 1, I-TRI CHLDROETHANE 1, 1, ;c:-TRICHLOROETHArlE TR I C.~LOROETHENE TRICHLOR □FLUOROMETHANE VINYL CHLORIDE CHLOROETHANE CIS-1,2-DICHLOROETHENE ETHYLENE BROMIDE LEAD, TOTAL I RON, TOTAL MERCURY, TOTAL MANGANESE, TOTAL Comment: s: I Samples collected VAL:ADO VAL:KCR at MW 2 ug/L ug/L ug/L ug/L ug/L ug/L ,ug/L .ug/L ug/L yg/L ug/L ug/L ,.1g/L ',.tg/L ug/L ug/L u g/l_ ug/L ,.19/L mg/L mg/L mg/L mg/L advise should you have questt □ns l'Respectfully' submitted, I ~'~Ll0,~~ ~ .Laboratory Manager I I Not Det 1 Not Det Not Det Not Det Not Det Not Det Not Det 1 Not Det Not Det Not Det Not Det Not Det Not Det ·=· ~ Not Det Not Det /'Jot Det 0.020 '21. 10 0.002 17.50 concerning these data. 1 1 1 1 1 1 1 1 1 1 1 1 1 l 1 1 1 1 1 0.020 0.02 0.002 0.02 I I I I I I I I I I REFERENCE 15 I I I I I I I I I I I, NORT1·i CAROLINA DEPARTMENT OF NA"TURAL RESOURCES AND COMMJJN!TY DEVELOPMENT --~/.JION Of ENVJAOHMEITTAL MANAGEMENT -GAOUNOWA~ SECTION P.O. EJOX 27687-RALE:IGH.N.C. 27611, PHONE (919) 733-5083 WELL CONSTRUCTION RECORD Ref. 15 FOR OFFl,CE USE ONLY Quad. No. _b__{.i:~_..lk_ __ Serial No. JL?_:J.j:_j Lat..")~ ':l <, ()½ Long. (;O 5.~ Pc __ Minor Basin ______________ _ Basin Code ______________ _ Header Ent. ________ _ GVV-l Ent. ___ _ I_ : DRILLING CONTRACTOR _/1,'--' ,.,lcc,C~-c,l) __ ~G~-~R~l~·•~• "'='-( ="~,'.,~,_-,_{~' ll __ _ /YJ ,_. _ _,, r:t I •~~:ILLER REGISTRATION NUMBER--"-'-')=(~·' _____ _ STATE WELL CONSTRUCTION PERMIT NUMBER: I I I i. WE'.LL LOC!,TION: (Show ~ke!ch ol lhc lo•:cltion lE!IOw) -~j_J.£!1 o ,.: :_; c,ef'.f1-S:_i1-1J:i..-'.K S I ::, 3, 3 (Rc;:1d, Community, or Subdivision snd Loi No.) Cily or Town Sta!e Zip Code DATE DRILLED \;· ;).'-/--f{7 USE OF \'/ELL 7>r'li c_ju.__ TOTAL DEPTH 3 L/ CUTTINGS COLLECTED O Yes O No COES WELL REPLACE E>:ISTING WELL? 0 Yes Q{j i-.!o STiT!C WATER LEVEi.: ,)7,C,). rop OF CASING IS / ' 'i) FT. 0 abovE: TOP OF CAS1~;G: 0 below FT .ABOVE LAh!O SURFA.CE. Coun1y: DRILLING LOG Frum To r-orm.i tion Descri;:itiun ------------- ---··-•-·------·-··--··-------- --_GBfilE·) ;·:\·-.,)J. i·· :;._s..;_~4-J~~----------- ______ fiL !. F_l.Cii.!, .. tU:.-.. -·----·- I:_ CHLORINATION: 0. Ct,SING: Type ;J;-i \\'all Thickness H additional S;)ace is needed use back oi form. I ;:rom ' : From Depth Oiame1er or Weight/Ft.1 Material ----To ____ Ft. ___ _ LOCA TIO,'/ SK.ETCH (S11ow direction and distance ;ro;,n_c.t leas: two State Roads, From . ' I , GRB\ci-Tc :1,itA1/t:rJ1I--< ----To FL---- or other map reference points} j l ,. I ~;}f, . -FF .z j,. s I I I I I From C Method p/'. :.ir.-r:c:: /,..',II, 'r) ,:JJ.·~·• From ____ To ___ Fl. ______ _ scnEEN: f7rorn ) Oeplh --'---To 3 V Lf f•i.Jm ____ To, __ _ Diameter Slot Si;,e /-!.a1eri11l 1 · ·,7-· .Pc•,' Ft. --------t>cL_ 1n ·&, 1-1n. Ft. ___ _ ,n ____ in.: ___ _ From ___ _ To, ___ F1 ____ in. ____ in.: ___ _ uTT:::.VE): PACK: C, ,.,, ,-.,((! Oep1h Size MateriJI Fro ni _s_,)"--'--1 •~\'--•-To 3 l/ Ft Fron1 _____ To __ _ r-t. ______ _ r, / i ,,, ;_ ( .. ';;,,,•-!, <.. .9EMARKS: -------------------~----------------- ! 00 HERi:8Y CERTIFY THAT THfS WELL W.A.S CONSTRUCTED Ir-! /\CCORDANC[ Wl"IH 1~-NCJ..C 2C, ','/[LL. CONSTRUCT1Qt✓ STANDARDS, ANO n-v~T A COPY OF THIS RECORD HAS BEt:N PROV,IDED TJ THE \VELL 01Nt✓l:n _ ~r;?,-::;;?2, __ J::}_<.ff __________________ ,'--C,· __ -~.:..l_-..c,;:..'_07 __ _ SlG:-M TURE OF cor~H,ACI OR OR ;...(;~r ,ii NOR1 H CAROLINA DEPARTMENT OF NATURAL RESOURCES ANO COMMUNITY DEVELOPMENT FOR OFFICE USE ONLY . ' DIVISION OF ENVIRONMENTAL MANAGEMENT -GROUNDWATER SECTION ' P.O. BOX 27687 -RALEIGH,N.C. 27611, PHONE (918) 733-5083 WELL CONSTRUCTION RECORD I : DRILLING CONTRACTOR 1 · DRILLER REGISTRATION NUMBER ---'-'-'"-'-'O'------ :1. WELL LOCATION: (Show sketch ol the localion belov:) I Near~sl Town: l_2 5;cirnvtJ> s,~p:t JC -,·~-i,uk ~ R 15.3 ·;; (RoacJ, CommunilJ', or Subdivision and Loi No.) OWNER $ + 8 +f I Re/£.isr·~~~----------------- City or Town DATE DRILLED ?, -::J ;· ·,\ 7 State USE OF WELL Zip Code Lmo cbs 14. TOTAL DEPTH--~--CUTTINGS COLLECTED O Yes O No ). COES W~LL REPLACE EXISTING WELL? D Yes 0 r✓o , I " STATIC '."/ATER LEVEL· >I·/ 1 FT. 0 above TOP OF C.,SING. 0' below TOP OF CASING IS _/_·.:t..l.___ FT. ABOVE LAl<D SURF /,Cc. I 7. YIELD (pmi IV fi METHOD OF TEST B/li: i WATER ZO,JES (depth!: ,)4 -3 '-I I. J. CHLORll·iATION: 1.0. CASING: Type Depth I From --'-'--To Wall Thickness Diameter or Weight!FJ. :,\aterial ,) 'I Ft. ___,,2 __ From ____ To ___ Ft. ___ _ I From ----TO---Ft. 11.-BROt/T: ' Btrv-fo,-.,,1-l. Depth Matericil 1 Method Quad. No. I 6 7 5 J_2 __ Ser;aI No . .Ig ~ f 7: Lat. 35 Y.3 Q;l Long. 8 D $8 ~f Pc __ . Minor Basiri _____________ _ Basin Code _____________ _ Header Ent. _______ GW-1 Ent. __ _ STATE WELL CONSTRUCTION PERMIT NUMBER: County: DepIh From To DRILLING LOG Formation Description I {: :: •.-~--~-· .. . \!:' r} : ; K 'P 'r.!,; ···-· ' ' ---£EP-:;r: -icJ:Jo-dT/o--·,."~"(.c:: ,,_;, __ _ II additional space is needed use back of form. LOCATION SKETCH (Show direction and distance from at least two State Roads, or other map reference po;nts) µ -ti; ~ 1'1 /5---s,pl ,", V : -(A,Jt.) 1-' 0 To ,2 I Ft. -~ ,"?~. 1/·./J /· .. ( P,~ ... 111/ ,-/ 4:;i-1.,,1 , ,:i d,l,.J From ___ _ To Ft. 1. :2 SCREEN· Oepih Oiorneter Slot Size :.:a;criol C we,) s· h "t ci From ____ To ___ r-1. ____ in. ___ 1n. Oep\h From .1 ! To _?, t/ Ft. ' t.-10Ier1:il :.::. S k JS33 I ~rom ____ To ___ Ft. ______ _ 14. REMARKS:------------------------------------------------- I I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTHUCTEO IN ACCORDANCE WITH 15 NCAC ST ANO,\RDS. ANO THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER. 2C. Well CONSTRUCTION ----·---z.x /2K. , s I , , ,<".·, ·_,,/. ,.J , ,,/,JJ!.-L , ~ .\d.. ____________ -'CL__c:::.._:_:c__:__~-- SIGNATURf: OF cor~TRACTOR OR AGENT o;,,TE NOA-fH CAROLINA DEPARTMENT OF NATURAL RESOURCES AND COMMUNITY DEVELOPMENT , ___ Qilll.SWN OF ENVIRONMENTAL MANAGEMENT -GROUNDWATER SECTION P.O. BOX 27687 -RALEIGH,N.C. 27611, PHONE (QlQ)·7J3-5083 WELL CONSTRUCTION RECORD. •--ORI LU NG CONTRACTOR -~f\/"'--'/?.'--'--'(---'[)L ___ -__..(~:_,_/<'-"-o-"u---'rJ-"-d---'. <c._•·'~,1'---J_,'---, r FOR OFFICE USE ONLY Ouad. No. L /, ? /} IR Serial No. ~CL Lat.<) Y3◊& Long.S0'Jo&pc __ Minor Basin _____________ _ Basin Code _____________ _ Header Ent. ______ _ GW-1 Ent. __ m cc-r:t-3 STATE WELL CONSTRUCTION ·=D=R=IL=L=E=R=R=E=G=l=S=T=R=A=T=IO=N=N=U=M=B=E=R=_=_=_=_=~l=O~O==O==========~===PE=R=M=IT=N=U=M=B=E=R=•;;;;;;;;;;;;;;;;;;;;;_;;;;;;;;;;;;;;;;;;;;;;;;-= I 1. WELL LOCATIQ/'J: (Show sketch al 1he location below) Nearest Town: _.clJcR~l',c,<c.:1L, _,co0,.1"w_ _____________ _ _ .bc,,ow,, I '>, /2J..-.1-'-I 0 ,-, [C SR I 3 o :,, (Road, Communily. or Subdivision and Loi No.) 2 OWCJER S,-/r:H ( c> ( 1)( DRILLING LOG I Depth From 1 o Formation Descri::.1ion ADDRESS------'-'-"'-"--="--'--'--"""-'-½~--~-~~-~-----lreet or Roule No.J I City or Town 2;:, Code I 3. DA TE DRILLED Y -) ) /' 7 USE OF WE LL Tc CD;° _.,. /-, \ - 4 TOT AL DEPTH 3 u CUTTINGS COLLECTED O Yes O No 5. DOES WELL REPLACE EX!STlr✓G WELL? 0 Yes 0 i✓o I 6. STATIC \',1ATER LEVEL: ];_I,;{" FT. 0 above TOP OF ,: . .:.SING. CR below TOP OF CASl1'~G IS __j_~ FT. ABOVE LAl~D SURFr.:t:. / YIELD [goml _ ___N_/1_ __ METHOD OF TEST __ ,3,e,-=-'-'-'--''---- I 'NATER ZONES (c'eo1h) ;J_ -----·-------·--------------·------------ I 9. CHLORINATION 10. CASING: Type Amount rV fl Wall Thickn'ess or Weight/Ft. If additional space is needed use back oi ium. I I I I I I I I 1 1. 12. :l 3. 14 From From From -GROO I.· iJ~,-J-lcr,u. From From SCREEN: From F1·Jm From Depth Diameter !,iaterial -~-'---' __ To _,2:L_ F 1. -~;) __ _ ____ To ___ Fl. ___ _ ----To ---Fl.---- Deon, Material Me:hod LOCATIOI✓ SKETCH (Show direction and distance from at least two State Roads. or other map reference points) n ~l:ll ,, 3 ~ I • - ~ '----s er \-' ' ?,--1'~ -~(~)__ To ,) 2 -0-Ft. ~*'-'"'---fi'"-'-lc:_'l'-'t lee>,___ __ yc,-~•,-c{ I dld...B.fPf--, • 1 ' {) cl d r-~ ____ To ___ Fl. ______ _ Deptn -~;)~'--/ __ To S Y Ft. :) s101 Size :.'.a1ericil To ___ Fl ____ in. ___ :in. __ _ ____ To ___ Ft. ___ _ in. ___ lin. __ _ C ' . I "Tli.~' lJ. fl ~A.-<. (L -PACK: St1,VC Size ;)). (__, Deplh J'-( From_~To i11•'. Ft _ _f_Y/fc( From To Ft REMARKS: 2C. WELL COl·JSTRUCTION I 00 HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15 NCAC ST ANDA RDS AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDW TO THE WELL OWNER. . __1~ WI .c,-?t-,''7 s1G1,A r:c.E o'-'F"','--:0-1-nuc,_;"_~~-,Lo_R_o_R_A_G_E_· N-1--------□~,--T-E-'.L---"---'------ r-1,1_, r, ___ , __ ., , , ,,., , I I t'0RTH CAROLINA DEPART/.1,ENT OF NATURAL RESOURCES AND COMMUNITY DEVELOPMENT DIVISION OF ENVIRONMENTAL t-AANAGEMENT -GROUNDWATER SECTION c..---'7.0. BOX 27687 -RALE!OH,N.C. 27611, PHONE (919) 733-5083 FOR OFFICE USE ONLY Quad. No. l,.. (, 7 c1 Lat.3t; t.l'., C'l· J 15 Se,;a1 No.J~C '//.) WELL CONSTRUCTION RECORD I I. DRILLER REGISTRATION NUMBER I ~ 1. WELL LOC,\ TION: (Show ~k81ch of the loca1ion below) 1 Necres1 Town: -,RWl~,'-"I f\rJ c-)' < . .--c J.. . -·-· ~ \h( '.I._ ...:... -__,i;f11 \ C_ I -r\l..)f -.. . .tX \\) \. "-.J \ I (Hoad, Communi1y, or Subdivision and Lot No.) ... 2. OWNER ~I k.CJ) · <~,R,w...il::,,_,_,q-,'i,. ADDRESS \.' C) \:,('i-; .-i .'7G 8? (Street or Rouic h/o.J (:,\1_C/C:M 1.:.i.c. I Cit~' or Town Zip Code I ]. DA TE DRILLED-~P"'-1..L..· ~2_:.;_··--2,7 <t. TOTAL OE::JTH ~~~) <, CUTTINGS USE OF WELL I, en\\ {) b COLLECTED O Yes CB No 0Yes Gt-10· 5. COES V,1E!_1_ REPLACE EXIS~WELL? G STATIC \'.'.:..TER L!:'.'EL: ~. .· FT. 0 c1bove TOP OF CASING, I J , 'I' [St below TOP o::: CASING IS ____l_!L2___ FT. A801/E LAl·iD SURF ACE I ·7. YIELD Igoe-.) -~-)_1_'/_., __ /AETHOD OF TEST \'/ATER ZC:-lES (death): I 9. CHLORIN;..,1101~: · o. CASING· Typ~ s {:-.. '. u \-'_ f!,:\ ,ct, (~-- I.J//\-Amount l l / (', Wall Thicknciss I From From Depth __ o __ To i.=r Diameter or Weight/Ft. tJ.aterial Ft. 2.1..._; ----TO ___ Fl ___ _ ----To Fl.---- Depth r.laterial fl,ethod Long. Re 5, C ~ Pc __ Minor Basin ______________ _ Basin Code ______________ _ Header Ent. ________ GW-1 Ent. ___ _ STATE WELL CONSTRUCTION PERMIT NUMBER: County: Dcolh From To SEP DRILLli'~C [_QG Formation Description --~ ---------- ~+--------- LOCATIOi·; SKETCH (Shov: direction and distance lrom al le2s1 1wo Slate Roads. or ott)er map r1ference points~\ i ,...----,--, ·-;, ,-, I / To ,..:....:·• -. Ft ,,_, c: ~:\\,;\.:; ~\-.,,; ·~-VI kJ/,'; /~·fl 1 '1d/r .(- ...f'.\'· 1:. " '! !'D, / I . 2. I 14 I From ____ To ___ r-t. ______ _ SCREEei: Oeoth Diameter From ·, .:; To :•,q ___ Fl _-.-~,~•--_'_in. ,(>.: ;n F1Jm To ___ r-1. ___ _ in ___ in. From To ___ Fl ____ ,n. ___ ,n. Frorn ____ To ___ Ft. ______ _ REMARKS. ________ _ M2ter1al I, ,_. ' '1_j \,J t'l ~'J :'! : ·:, r,_, .. _,:.J:'." :..... -- I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED lt-J ACCOROAt-JC:: WITH 15 NCAC ST.t...i✓OARDS, ANO THAT A COPY OF TH!S RECORD HAS BEEN PROVIDED TO THE \'/~LL OWNER 'N[LL COi·lSTRUCTION _1~'i I,, 1,ki~/ __ _ SIGNATURE OF cor-JTRACTOR OR i-.Gt::r✓ i I I I I I I I I I REFERENCE 16 I I I I I I . I I I I - - -------------- - I 7 2 3 4 5 6 7 8 9 10 1 12 13 14 15 16 1 1 2 8 9 0 A B C & cor(,)N1TY. -- REPORT rO: ARO, fl!O.(f:H1Q') l!RO. WnRO WiRO WSRO TS Other __ (_\_·,_/_•, __ (_i_,_,_:_.: :._··_,_••_· _·_· _· ·_· /_._·:_•.,_' --.,-----,-.,-~ Bus. 1c-;-~;·ier)other -------------,,-___ .. :_,. ;':f 9, Shipped by: (Qt l EC l()llfS): • I -r (l,,.d!.J-1 ....... BOO RANGE• 0 I It J ·• N Cl: .. ,,,/: PT. OF NATURAL DEVE[OPMENT .,DURCES lAS.NU/.\!HR 00008: DIVISiCJN OF ENVIRONMENT,\L MANAGEMENT WATER QUALITY FIELD·LAE St.MPlE TYPf FORM (OMl) 0) Rec'd by DAIA ENI RY BY:' □EMERGENCY . ,-fie.~"> .. STATION LO(Al ION: {·f.: .• ,.. OsrL11 -L, .. OAIF Rf PORTED· / - ? :;· '/ 3 [,! J J . >--•>n,:. '20 ,-::-✓ (: / ·,:.>.REMARKS: s~<,n,f/c. ?Jee• o,iq 7Z:l:~., .-jJv~ -!..-1-<c ,.,,/:lJL Ll~!j le. . •."1 w/:c/. '' "~ --~· 'V /4 /, I,;, '/ -Siution Numoer ,., t ---· :::._ I ,._L. _J BOD ;uo - COD HiHh J•!O COD low J)\ Colito,m: IM Fe col Jlt,lt, Coliloun: Mf lo!ol 11"-04 Coliform Tube f,:,<ol 31615 Coliform Tube lotol 31505 Ru1iduc· lotol M Volatile SOS fi,ed S!O :'.:.' ' Re~idue ·S end<'d 5.10 Volatile 535 F ·~ed ,,o JpH 403 Acidi1,,, lo i,H 4.5 •36 Aci~ 10___1::H 8 3 435 Al!-.olinit1 tooH83415 ~1_!-.oliniiy " pH 4 S 4H) ~- ,----10( 680 Tuibidity 76 So,nµling Point 'Noler Tamperalure("Cl Pl 1: 6 Seuhi (Me!erl} 78 l H,. SellleC;,~\e Molter (ml/1/H,_\ 50086 OM 1/ Re~i1ed 7.55 10 Ai, lempcrolure ("C) 7D Deed fi1n Sev<'r ity 1)40 iirr,c Begin D01., ''" 1J''':JDe,,,h OM DA l)Br.\ Value lypc Dote Oeg,nfyy/mm/--/ " H l !T7 t.J3 _I ,'.)i-/ J !..' (·,, I mg/\ Chlo,id~· 940 !W~(I NH7 OS N 610 n'9 /I rnq/1 \.-~ Ano:nic Jolol .1QDJ. :,:·i,:.· u-;_/1 IKN o\ N 615 n,!1.{J m<:i/1 Chi 0 Tri 32217 ug IJ N07 .. ~~01 01 N 630 mq/f 1100ml Chi a: Co" J 220'} uc /I ro4 OS p 70507 mu/I 1100ml Phe9£.b.y1in o 32213 l!_li/1 p, ioiol OS P 665 mg/I /\OOml -Color: i,uc 80 ~ --Pr-=-Co r, DiHolved OS P 666---mg/.1 ,,.:) .,~~ -.. :;:"" . ..-' ug/1 1100ml Chromium: Hex .1037 U9/I )( Ag -Silver 1077 /.t./r ~)00 ,;,,, /I )(' -Akminur,, 1105 vgll Cvonide 770 Al mg/I , ·ins/I( Be -Beryl!ivm )012 ug/1 mo/I F!uoride9:;,1 ·:f(f,.- mo/I Fo,moldehyde 71880 -. ii,q/1 Co Col<ium 916 mQ/1 mg/I Gree le ond Oih 556 mQ/1 ,· < _lt",) Cd-Cadmium 1027 .,.,_, mo/I Hordne 'ii: 10101 900 m4/I Co Cobell 1037 uo/ I ... . -,-x •. ... , "..") m· II Ch,omium:Tolol 1034 ug/\ mo/I MBAS 38160 .:;: ::.-~o " Co~oer 104? vq/ I · "u, 11 ,, Co units Phenol\ 32 730 m!=J/1 Sulfate 945 •l_l_9_l1 :< Fe-Iron 1045 . //. .,),) ,:; ~9/I mg/I Sulfide 745 m,ifl X Hq ~ Mere u!..l.J ]900 o .. \~ u,all ' mq/1 Spe<ilic (and. " uMho1/,n, Li -Li!hium 1132 u_g /! -:,:-J // ' ) ·,.,,g -M1;1_9._nesium 97 7 .......51_{_1 mq/1 Biomon: 0~ Wt. 573 9/ ,',\ -.. 35(> ' / mg/! BiomcH: Pe.,i Ash F,ee 572 9/,.i Mn -Mcnqonese 1055 ~_{] ' :<I No --~,· ~.-j m!,111 NIU Chi o, Pe, i Fluro B754 7 mg/,\\ Sodium 929 pH Cond.,ctonce AH,?linity 0.-.,. 01 2s·c PH 8.3 pH' . s j, !. Joo 400 " 82244 •131 P,ecip1!clion( l':'/Ooy) Cloud Cover. ' D.0. -,;. So1J,01ion Salinity <t. Algoe:Flool!ng MoH Severily ' 301 480 132 5 " " Odor;A1mo1phere Stream flow Delergen1 Su<1s Oi1-Greo1e Turbidity Severity s~verity Severity Severity Severity 13 50 1330 135 I 1305 \)00 Compo,i1e Somplo Typo ' s 8 C G GNXX .· Ni -Nickel 106,' ---:·. ,:;-o u<1-' I (_i :, .-., l'l,-t,·,1<l 1051 "!lil --- Sb-' - Anlimon'[ 1097 vu/1 Sc-Scluniym" 11.:7 l"\J." I ---- .'-< Z.n-line 1097 ---· :.·) C)U u,1.-I ----- - . ---- Pe5ticidcs S □ eci!icollY Scon Oi:._goncichlorlne Scan Organopho~hor•Js x Oraanics Speci!icol!_y t Scan Bo~e I Neut re! Extroctoble~ ) Scon Acid Extroctoble~ r SpeClo! Anolr~i~ Sp_ecifical! ~~\\J..,. _ _:__~i_ '() o, -"''M Scan -Ac~;~..- x;• ~-S.\1n -IN~ les Acidi1y PH 4.5 PH 8 J 87243 8174 2 Wind Oi,ection(Deg .I Wino For<c Beoulort 36 37 ~ Flooling Oebri1 S!udgo S"vo,i1y s,.verity 1)4 5 1)15 1· _ Rep~rted by 1 /Y]} Checked by C ,A I S_upervisor ']('f,t'., ORGANIC ANALYSIS ~utered b~ ~( I I I I I I I I I I I I :1 I I 1- 1 J_ Lab No, 7q 3C!? (/ .. Checked by I)f Sample Type : h Jez_ -/o // Analvtical Results ,/~ /Jt!,,. ~, -r ,./4__, I , ,. r\ , 4"j 1.J~./.: /,._, --½il, , ;:r:;;._✓ ·L:. 'f) -, --__,-1"1-r--,:I' ;¼uJ / 5/" :-----;;-/7_ I y;;:, ~ --j-;; / _/ / ltlll/f~...._• _.... - r ✓ -h:. r-, -I,~ () A~--,7#/ /, _.,.--/ /.., .--,1-;_;_,, ~~ ,4_ ~~Jl /)7.,-/ -..I ' A nft_,p /1-r, --r,; , ,,,-;,,,..,.,;~ ~ /) (),; ~ . , / -;<--' -/~// /,. / ~ ,.:~ n-/:( Ji.' -'~n 0 .J;o I _ /. '/ / ·- _.,. ✓: -, _.) , J!. /°) 'oA.r , .L., 1-.o -~ _._ .,. r ,,,./· - ""J'&JI ' 'I lo -, -~" ' .. l, (/ ,f 11_ .,I /, l, jl_ ' /} Lin.,._ ' I, --1-""'",,_ i.1 p /.' ' ~ .,,../... -± -/2-: I /~ I I~ c/,,;., c ~--()•*· ;;t._f ~~*-, ' , ' ' ' ' ' ' I GC/l-15/DS ,.1sed Concentration J - /,,y/f , V ; /d ✓-:o ::Z9 /"'/c <C:: /7 --< .) -</0 /->00 I I I I I I I I I I REFERENCE 17 I I I I I I I I I pnm1,-,,. l'if255Cf71 .I / I I I 0 State of North Carolina Department of Environment, Health, and Natural Resources Division of Solid: Waste Management P.O. Box 27687 · Raleigh, North Carolina 27611-7687 Ref. 17 r.es G. Martin, Governor .illiam W. Cobey, Jr, Secretary William L. Meyer Director Septembe~ 14, 1990 TO: Mr. Keith Masters, Western .>.rea, supervisor Hazardous Waste Compliance Unit' FROM: RE: Kr. Scott Readling, Waste Management Specialist Hazardous Waste Compliance Unit: Site Investigation of .>..A.A. Enterprises, Incorporated, Sigmon Septic Tank located in Statesville, Iredell county. On Wednesday, September 5, 1990 a;visit was made to the A.A.A, en~erprises, Incorporated Sigmon Septic Tank Company located on Eufola Road in Stateville, North Carolina (704) 873-8954. Present during the visit wer~ representatives from the North Carolina Department of Environment, Health and Natural Resources, Mrs. Christine DeRoller, Hydrogeologist with the Division of Environmental Management, Mooresville Regional Office, Mr. Steven Clayton, Environmental Supervisor with the Solid waste Section and Mr. Karl Shaffer, Waste Management Specialist also With the Solid Waste section. The purpose of the visit was to evaluate the site and determine regulatory compliance under the Resource Conservation and Recovery .>.ct. The request for the Hazardous Waste Section involvement came from Mr, \Karl Shaffer, Solid Waste Section, Septage program. Mr. Shaffer had been aware of the site and had been overseeing the operations and as a result of new regulations the existing site I would no longer be used therefore closure of the site would be needed, Closure of the site would be dependent tlpon materials present or absent f.rzm the surface impoundments located on the ·property, Mr. Shaffer requested the presence of the Hazardous waste Section 1in order to give the owners guidance with the sampling procedures and other requests from the department which may be necessary for closure, Results from groundwater samples collected from the property by the Division of Environmental Management on June 14, 1990 indicated violations with groundwater siandards for Iron and Mercury as well as the presence of other constituents such as Lead and 1,1 Dichloroethane,(SEE .\TT.>.CHllENTS) The Sigmon Septic Tank Company i• ,owned and operated by Mr. Henry Sigmon Jr. and his sons. The operation !eludes the pick up of septic materials - ( ,,- •: ! I mainly consisting of wastewaters from various industries located around the stateville area. These materials are transported and diiposited into a total of six (6) unlined surface impoundments located behind the business which is also located in the basement of the owner's residence. The practice of depositing of such materials in this minner has been carried on since 1978 or 1979. Two (2) surface impoundments have been closed out to date and are identified as impoundments numbers eight and nine. Surface impoundments identified as numbers seven and ten contain water run off from the existing six (6) operating ponds and are connected by a septic T, the waters collected in these two ponds are used for irrigation purposes. All of the ten (10) . ponds are appoximately equal in dimensions which are one hundred (100) feet long by twenty (20) feet wide by ten (10) deep. Four (4) groundwater monitoring wells three down gradient and one up gradient have been installed by the Division of Environmental Management about three years ago and are also indicated on the diagram. Hrs. DeRoller indicated that the site does not have a nondischarge permit or. a NPDES perm!~ ana that the site was orginially opened and permitted by the county Health Department. As a result of the evaluation the proper closure of the surface impoundments cannot be determined until laboratory analysis indications are shown, which may indicate either the p~esence or absence of hazardous waste or hazardous waste constituents. Hr. Sigmon indicated that the company did rrot knowingly transport hazardous waste or :any hazardous waste consitituents, however did indicate that the facility idid have an EPA identification number NCD062555792 and presented it to me. No record of the company was shown on my list of facilities located in Iredell county indicating an invalid number. Any followup action by this department iia pending sampling results from the surface impoundments. Requested sampling requirements were stated to include the following: At least three (3) samples per pond to be taken at various depths, surface, middle and bottom sediment to be analyzed for volitiles and for the presence of EP Tox Metals. SF I Diagram of Ten (10) Surface Impoundments located at the Sigmon Septic Tank Company as well as the location of the four (4) groundwater monitoring wells • I I I I I I I I I I I I I c ______ 10 __,J l 2 3 4 5 IC • £:it.1-:-T1t-Jt.. C.P.01.Wt>lll"~ MowtT;R:,tJt.. ~E!.LL hJ-E.TM•Pb 8 • ' j • 6 7 9 • [ ' ·r--· 'I .J' ::c (I) . j ,..., : I O 1 I ! -J, I I I I I I I I I I I I I I I I I I ~~ ' REFERENCE 18 ' ' • · ,JuAo .,o. C67n-7 ~AT 1~0 rb' .v" Rupori lo: ARO, FRO, SERI AL NO. vo' :;g / /?. ., LONG, ~ ARO, WaAO. WiRO, ------ - NA I URAL. KESCJuKCES ,c11~1/'NNl0Y~ru§raoy GROUNDWATER FIELD/LAD FORM 0 SAMPLE PRIORITY WSAO, Kins1on FO Shipped by: BuS, 0th er _________ _ D ROUTINE 10:'r'O TIME~ D ·coLLECTOA(S.J: --<tt,'-"'CL+iL..--DATE FIELD ANALYSES DH ◄oo ---Soec. Cond.94 ___ a1 2s0 c Temo.10 ____ 0 c Odor ______ _ Aopearance ______ _ Taste ______ _ I ;eld Analysi_s By: ____________ _ LABORATORY ANALYSES 800) , " mafl ---------coo ,uoh ,.o m9/I COO lo• JH: m C' /I V Colllo1m:Uf F tc al J 1 6 I fi .: I / 100ml Coll1ium:UF To If I 31~0' / 1 00ml lOC "' i m9/I 1vrb11111 r " 1/lV --'" '" vnl11 Jd\allnllr 10 pH ◄.~ "' "'Q/1 Allllinlly " '" .., ., ' m C'/1 C1rbon111 '" mer/I Blearvor111, "0 moll Ar_unlc:Tolll 1002 v,;ifl C1rbon dloJld, "' moll Crdo11dt ,~o moll Ch1omlvm:Htl 10)2 u "/I Color:Trvt 10 PI ·Co Cp nldt 120 m;/1 lab Commenls: EMERGENCY PURPOSE: BASELINE. COMPLAINT, COMPLIANCE. Lus··-~ B1. .:X:nu.· (circle one) _,.., Owner .4 lle r Localion or sile , 3 ,,.,. fr; Description ol samolinQ polnl well Sampling Method \r\--~l-(,,,~y (pump, balle"r, e1c·.) Aen,arks J),,,,1r1yodr/r7..f.-. cf 9;12t"-fP f?nuJ. < ~•ell [s·;y,noos ► obc T<vJk 7 ' urn. Solld1 IO J IJO -mg/I -Ao Siha, -1011~ Fluorliu '" moll Al ,.,,umlnvm I 10 S H11dnt11:lolll 900 m Q/1 •• 81rlum ·1001 HHdntu {non·, 1 r o) "' mo/I ·c, c,1,1uni . " Pht 11011 J21J0 \IQ/I Cd CI d~lvm 1017 Sptc:lllc Conll. " vl.ll"loS/,ml Cnromlum:10111 IOl ◄ Sul I 111 ''' mo/I Cu· CoPotr I 04 2 Svlllll t :Hs ! . ·:~<i,Jn f. · Iron IOH ; , Ho · u,,cvrr 1 1100 ··-···· K • Po1111lvm ll7 ' ., ' •1"1'11 I.lg· l.l1gn11lvm IZT . 1 ' •:~-I ""' l.l1ng1n111 1055 "' Sodium 121 ti HJ !'.<if<: i:,;; ! : ; · .. ·.!. L'.i'. .. ~!fr. IKN ., lti; H~~. L..::. I.ad. .:nc eil:.\Jt,:' NI NI, II. t I 10157 Pb l11el IO~ I NOJ ~ NOJ " " 6JO mo/I s, Stltnlvm 110 P:J 0111 " p '" ffis'/1 lo 21nc 10'1 . ;,,-07' -5..0--.x>e,y si,,,k5v, lie ,PC ..?86 ?'.> of I 13B Sample In I er v a I __ C<..,,"""'-' /£.. _________ _ /c, CA-f"' r-1 C J (pumping lime, air lemP,. e1c.J "'""' '-f' 3 'r'. .;}4 J ·--vo11· Ol111nOCn1;,;,.,, Po I,; t • 0 o I u;n 0191 no 111> o 111 no,~-1 1' I II• Cl O O I vOII m;/1 Acid H"Oicidtl VOi' 1 volt a 11 • ' ~-ul11 ,r £,11,c11011 0 r 9 I nl t I uot1 ... t Id f,;/uu011 Qt; J "'Cl votl UQ/1 v ,v,1;1,101, o,,,,.,;cs (·~QA o o tu, J mgfl m.,, I' 1 Oi01omo11,.,,,,, IE JS J vgfl mi:,11 VQfl \ I VO /I ,..,, \ I .,, ~.,_·u•,.r vo II v11fl ·-, GW·S ◄ ReviSC?d 7185 ror Dissolved Analysis · sui.;~nil filtered samoll! and wrile ·01s: in block While copy -Headtluarler:: Pink copy -ReQion Yellow copy -Lab .-:: -· ·-0. I, I I I I I I I I I I I I I I I I I I VOLATILE ANALYTICAL REPORT LAB NO. IGI02 REPORTED BY ~ ENTERED BY CHECKED BY ¼;_£) CHECKED BY REVIEWED BV u ' SUPERVISOR 'Xe.K DATE i/sh1 SAMPLE TYPE: WilTER ANALYSIS RESULTS STORET HO. COMPOUND 391 80 TRICHLOROETHENE 34475 TETRACHLOROETHEHE DETECTED BY GC/ELCD. NO VOLATILE ORGANIC COM~UNDS DETECTED BY GC/PID. hd, S)s CONCENTRATION 0.35 UG/L 0.29 UG/L - --11111!', V ~ - - :~~UMB:-: ~~7-d,~.' --Otf A O NO . 1.1.J_fl:.2_ S EA I A L LAT. ·)~'-'y-::_i' )7'' LONG. NO. «<t :5':'/,1 '' Department of Environment, , ,ea Ith, and Natural ResourcfJs I ''I~ qr r, 'Le=: DATE RECEIVED 1/, ~ J;me '-7. -,/ Division of Environmental Management 5 Groundwater Field/Lab Form Rec'd by: D From: Bus~ Olher ----------------CHftb~~iGf fRld~,tf1 ny DATA ENTRY BY: WSnO, Klnslon FO 0 the r ________ _ □ ROUTINE □ EMERGENCY 0 WV CK:~ DATE A E PORTE O: _,._/_-"'8'-----_,_Cj-"'_J/::..__ __ _ .-------e, Shipped by: Bus(Couriei; O!her _______ _ COLLECTOR[S): -,~721 ( f•' OATE II /13/?1 TIME ,, us PURPOSE: BASELINE, COMPLAINT, CO,..PLIANCE, LUST, OTHER (?,·, (circle o~) FIELD ANALYSES Owner (l I le,' ,6'(.J,>; c?.5·7 Sh le, v, lie -~< ,'./f,< 27 • '>,•y -J : ~ ,t: I :~-x pH 4 Qo ___ Spec. Cond.g4 __ al 2s°C 10111D, IO ____ OC Odor ______ _ Appearance ______ _ Taste ______ _ Field Analysis 8y: ____________ _ LABORATORY ANALYSES 8005 :)10 mg/I ----coOHlghl ◄O mg/I COO lo• '" mg/1 Colllorm:UF F ,e,r J 16 1 6 I 100ml Colllorm:J.IF T 011 I l 1 ~O ◄ /IOOm\ TOC 680 mg/I T u1b I di ty 76 HTU '" "' uni 11 Alk1llnll1 lo pH ◄,5 "' mo// Alkallnl\J " "' '·' "' mg/I C1rbon11,-... mg/I Blearbonlll .. , moll Arunle:Tottl 1002 .,,,, Carbon dlolldt "' . mg/I Chlofld, 9◄0 moll Ch1omlum:H1i 1032 ug/1 Color:Tn,. 80 Pl·Co c 1,ntd, 1 ,0 mg/I Lab Comrnenls: L oc a I I On or s i I B -~·-7~'1.....-'-'~'0.:..:_· ~'(-~'L;; _ _:[L-L' .C•'~•~'Y'-:.:__~.,.~-~,~f?_._'-. ___ "'CL--"-">.1.--'---'---'-""-"--"'----''-"---'--~ ;oov 00 d,·,1 ;C.: <· ;,:, '>o..,fl_ "6' s J. 13 _,~ / Descripllon ol sarnolino point T SamplinQ Remarks Me I hod /)-..,re{-(-v-JYttnp, ball~. olc.) S amp I e I nler va I _ _:C,c£'1..<L _________ _ )_J, > c :cfe,, f fl _5 '( d-;;, Olu. Solldl TOJOO ~g/1 F luo1ld1 951 mg/I / Hudneu:ToUI ,00 mg/I ,,,. H11dn•11 {non-cub) ,o, moll " Ph1no11 32 7 lO uo/1 ,/ Speelllc Cond. " u1Jho1/cm1 \' , su1111, '" mg/I Sull1d1 1" mg// X < \" ,. \' 1· ""' .. H 610 mg/I I' TKH .. H 625 moll No2•N0311N "' m g/1 P:To1 ■1 11 P 665 mg/I _Ag_:_Sllvar 1 071 -,, • Aluminum I I OS ,. -Barium 1001 c. C ■lclum . " Cd Cldmlum 1027 Chromlum:Tol■I 1034 Cu • Copp11 IOU F • • lion 1045 Hg -u,rcu,, 1 1900 K -Po1111lum 931 Ug -U1gn11lum 927 "" -'-C1ng1n1u 1055 "' Sodium 929 HI • N le k I I 1061 ''.f,. _,,. ,. ·t ., (pumping lime. air lamp, etc.) ug/1 ----O ig-il1oChl orln• ·,., ,11 cl du ug/1 Oro1nooho■ot"1oru, ,.,,tlold•• .,,,, mg/I Acid H11dlcld11 ug/1 ug/1 e,u / H1ulr1I E1lraclabl.1 01ganlc:1 uo11 A.cl d E•lr1t11bl1 Organlu ug// ug/1 I)( Pu1g1ablt Org111lc1 {VOA bolll1) moll m.,I I.?• Olbrorno11han1 (EOll) ug/1 mg/I ug/1 C'~ ll.lf .. -~,.~A.NI~ ug/1 ' .IN.I ~"-IQ O<PrlRT ; ug /I ' -.. I ' ug/1 V I For Dissolved Analysis ~_subr; · ,lored sarnplo and l--~01s· In block Wliltn r:nnv. t"lrnnn..tw~!nr r.,.~:-.1 (")fflr,. Ynllr,w r,nnv. nn11!nn;1I nlflr:l'I 1-·.· --·i • i I'. , __ I I I I I I I I I I I I I I I I • .............. r...-..-......... :.c../" '-'1', I C.U t., i i I .... GHUYE[> BY rd:\i ['w'ED B'l ,AMPLE T,'PE: VATER CASi4 \/OA T dnJet. Comoourid 7::i-3j-4 l , 1-Dictr ioroethH1t' 75-09-~ :Mf-t.hw lene Ch 1orid\: 1 5':--60-51 tr ans-1 .2-Ciich k>roeihene 7~-34-~ 1 , 1-Dichfor·~th<lrH:' 590-20-7 2 .2-[l;ch 1oroo,-oo ane 156-59-4 cis-1 ,2-Dichloroeihen.e 67-6£.-~-Chloroform 7 4-~7-5 l 8romocn loromi:-Thani:- 7: -55-6 l . l . 1-T,-)0hk,r0t'th-2int" 56::'--':·8-S 1 .1-~1ichl,:,roproN-nE- St,-23-5/Cartu:in T >:>tr ~chloriu':' :01-06-: 1 .:-DicJ·,tor,Jt'th.:ir,t' VDL.6.TILl:C "'-NA.LVT"IC•L 01:DOQT Tul ug/L 0.7:5 0 .2:. 0.75 0 ~e -'~ 0.25 0.25 o.:s 0.751 0 ""•C" .LJ ! o_:5 1:,_75 0 ,e -, I ,.., ,,...,.,..., ,,,.._,.,,n ..:,ur t..:.r,,· 1.:·Ul'. ~~--,- [)ATE : ENTERfD BY ,----.'-'LL-Uj.J""'-1 CHECKED BY --=M--'-"== ANALYSiS RESULTS Cone ' CAS" De\ec\ed MS uo/L ' ' LI 56-18-4 VOA T dn;it-t Compound 1 ,:: ,3-Trk·hloropron;.nt' u 1, Q'!::-BE.-1 1iBromoben::c-ne Ill I 95-4 9-812-Ch loroto JU('M 0.57 ' 106-E-4 4-Chloroto lll<'n.e I 541-TI-1 1 ,0:-Dicll lorobffisen<> D u 106-46-7 1 .4-Diclllorobenzene D I '35-50-1 1 .~-Dii:.:hl,::nobt:n:ff1E- I LI %-12-8 1 .2-Dibrorni:,-3-Ch lor0cirooani:-! D ui i ; ~:0-82-1 1 .2 .-;.-Trii.::hi0rubt"n.:ent" I LI 87-68-3 Ht-x:.Eich lc,r,~,t,1..it ::dit-n,:- UI 87-61-611 ,2 .2.-Trii::hloroi:,':'nlo?Of:' i u: i cz~-o"t-4 Mo:thlJ }-te-,·t-butt: 1 ft~.tr TOL Con,:.: ,,g/1 De\ec\ed uo/L 0..25 I 0.25 I 0 ~e -'-~ 0.25 D 0.25 1.5 f''I ',C _, __ _, 0.3 1 0.25 (1_·:,5 Ci 75 I ~ i -·. 7'?--0~-6 T~chlorc":'+.h':'n.':' 0.2'5 ·1 0.89 I 71--43'.-2 B~nz.':'rt4? I D I 70'-0 7-511 .2-Dich iorooroo<tr11? I 0.:25 I 75-:7-4 l 2-rwriodic:h1•:,rome-~h<ti1€-0 ~e -~ I 7 4 -·~5-5 ! [>ibnHT11~1mJ?t h<1n1? I 1 I r 0061-01-5jci;-1 .3-0fohloroproot"nt' 0.25 h OOE. 1-o:-E.[~r:ir15-\ '!-C'ich lor-op-roptn? 0.25 I 79-0(1-5 1 .1 ;2-Trlchloroetl)~ 0.251 127-18-4 T ~tre1c.hk.rvi-lhH11:" 0.2:: 142-28-9 1 3-{)ich1or=opane 025 124-48-1 [,i!,romoch loromethane 0.75 106-93-4 1 ..2-Dibromoethcine I 108-90-7 Chlorobenzl:'n':" 0.25 630-20-6 1 1 , I ,2-Tetn,chioroe-thane 0 ,,,, ~~ 75-25-2 Bromofor-m 1 79-34-5 I .1 .2 ,'.:'-T e\r •chloroe1hane 0.75 • TOL-~ar~t quantibffon limi+. T-tentatively identified compound [-e-!timated YaluE- U:-compound v •t •n• ly 7.M for but oot detected N-r.ot .,nahjzed for this compound V-Ot1-t.~ted ~lo-w qu.;nthation limit i1S-;.:,;;GC/i-!S .sr.<1olr-:tsis pe-riurrr~d Lil !,u IJI U1 u UI 0-53 ! LI u IJ fl u LI u TOL !-ubj~t 10 change dtJt:> to lll$trumffit :;-e,n$it?vity COMMENTS. 108-88-311 c,lut-nE-I I 1 ; 00-41-4 Eth1Jl t•>:ii::t:-rio: ; ' 1 108-~8-~ m .D-X•J IJ?nf:': , I I 5. I i 95--n-o u-XulH1t' i 1 1.3 I 100-42-5 StlJ ren1: 1 98-82--8 lsoorO()(J lb>nzene 1 103-65-1 n-PrVDlJ llif.n.::ene-1 I 108-67-8 1 ,3 .5-T rlmethu lb-?nze-nl? I 98-06-6 tert-Butu !benzene I 95-63-E, 1 :Z 4-T rimethlJ lbE-Ozene 1 D 135-98-8 sec-Butu lb•nzene 1 9'1-87-& p-lsooropu Ito lu;.ne 1 104-51-8 n-8u-t:1,J lbe-nz:e-~ I 91-20-3 Nanhth•l•n• 1 Cunc other purgo>blec (up \o 10_ higt,.,,-t p••ks) D•leeto><J u9/L · ONE UN ID£NT IF IED P£ AK DETECTED 8Y GCIELCV. ~ FCnJR UNIDENT1F1£[, P£AKS ,,.-,----- "vt.lt.L-lc.uB'r l>l,/r·[.,_ ( t12\ ui i l ~i l ' ' IU I_ i ui ! I_I ! u: ! I ! l) : I '1 I_/ i I I :1 I : ·-~ I I ! I U \ i I " j I I·-' i ' i I i I I : 'J ! iu u u u u IJ I u lu I IJ I I I I I I I I I I I I a I I I ' . ~~~ci'/ .~; State of North Carolina Department of En~iron~ent, Health, and Natural Resources 512 North Salisbury Street • Raleigh, North Caroiina 27604 Division ofSolid Waste Management James B. Hunt, Jr., Governor Bill Munford Rt. 14 Box 356 Statesville, NC 28677 Dear Mr. Munford: Telephone 919-733-2178 ' February 22, 1993 Jonathan B. Howes, Secretary ® Please find enclosed the analytical results of the water sampled from your well on Septernber;1, 1992. The analytical results of the water sample indicated that the following constituents were above the North Carolina water quality standards for ground water (Title 15: Subchapter 2L .0200): manganese (0.09 mg/1), mercury (0.007 mg/1), and nitrate (23.35 mg/1). To confirm these concentrations, the state intends to resample the well. Ms. Chris Deroller, of the Division of Environmental Management, will contact you about resampling the well. Communication with the Division of Environmental Epidemiology indicates that consumption of water with these levels of mercury and nitrate may pose an increased health risk. Pregnant women and infants less than a year old are particularly susceptible to nitrate toxicity. The concentration of manganese in the sample does not pose a health threat. However, manganese at these concentrations can cause staining of fixture and clothing. If you have any questions, please call me at (919) 733-2178. Ms. Deroller may be reached at (704) 663-1699. Sincerely, -:,1~7~ ' Laurie Martin, Hydrogeologist Ground Water Unit Hazardous Waste Section cc: central files Jesse Wells Chris Deroller, DEM PO. Box 27687, Raleigh, North Carolina 271Jl\-7687 Telephone 9!9-733-4984 Fax,# 9!9-733-0513 An Equal Oppom.Jn.iry Affirmative Action Employ,=r I I I I I I I I I I I I I I I I I I I -----··---------······ N.C. ucp.:irtmcnt of Environment, I h.::Jllh, & Nalural Resources S..1lid Waste Managc:-r:.:n: Division SA.¥1PLE ANALYSIS REQUEST Su1c Ubontory or Public Health P.O. Oas: 2..~7. 306 N. Wilming,on Stn::ct R.alcii}\, North Carolina 27611 .Site Number ----------------Field Sample Numbcr ___ __,~c.....=O:...:::J'-'=2=-------- Name of Silej'J6,..,v .<;("//le /;y",v4!K Z> Rf.fi'24f Location __ .,e£,c....:::Lfc.Cc.....,"::...:::Lc.:'1:,_ ___________ _ Collected By (0 ct5.r5/_.,,~77.,-,., ID#/ WV Date CoUected __ Lz;.1.6__:_l/_,/c__.c.1_.L-=-__ Time_..-/_{f ... ~__,C:.,'L.c. 1 __ / Agency: ~az.ardous Waste Solid Waste __ Superfund TCLP Compounds --. . Sample Type ' Inorganic Compound., Results(mg/1) Environmental Concentrate Comments Arsenic --Barium faound waler (1) ! -- _ Solid (5) Cadmium --Chromium -- Surface waler (2) _ Liquid (6) ' Lead ' __ Mercury _ Soil (3) _ Sludge (7) ' Selenium ' -- ' Silver ' -- Other ( 4) _ Other (8) ' -- i ---- Organic Chemistry Inorganic Chemistry -- Parameter Results (mg/I) Parameter 1: Result.s(mg/1)(~ Organic Compounds Resulls(mg/1) _ P&T:GC/MS _t/ Arseni!= <o. o l£ benzene -- --Acid:B/N Ext. V Barium o~ g :;;i,. carbon tetrachloride -- MTBE -4,.L;Cadmium (Q. Qlf chlordane ---- --_IL Chloride -<-S chlorobenzene --V Chromium (o. oy chloroform ---- --_IL_ Copper LD,c:,S o-oesol -- --V Fluoride L...o. I 0 m-cresol --!/Iron i 0.08 --p-cresol --2_Lead I (Q.O(J cresol -- --Manganese O.Q9 1.4-dichlorobeoune -- --~ Mercury o. Qo 1 1,2-dichloroethane --Nitrate ;:,._-=,_35. = 1,1-dichloroethylene ::Z Selenium < Q, Q.IJ_ __ 2,4-dinitrotoluene .JL Silveri "'-..o.o5. __ heptachlor Radiochemistry _JL Sulfate's -<:. l<,_ bexachlorobenzene -- ···-·-·· ~Zinc' L.Q-O:;) hexachlorobutadiene Parameter Results (PCl/1) pH I 6, (',; --hexachloroethane __ Gross Alpha __ Condu,ctivity '.d, q Ci; ,ll :s __ methyl ethyl ketone Gross Beta v TDS ?..[ l nilrobenzene --]z:TOC f:yv;a ~~I-,/_, l.r.!b __ penlachlorophenol I . __ pyridine --Microbiology --__ telrachlorocthylene --__ trichloroethylene Parameter Results (Col/lOOml) --2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----' __ vinyl chloride ' endrin --lindane Date Received Reported by : __ melhoxychlor ' __ toxaphene Dole ExtroctcJ Dale Reported 2,4-D __ 2.4.5-TP (Silvex) Date Analy,cd Lab Number -- ' ' I I ' I I I ' ' r,.c. o,p,nmcnl of Eovironmcnl, SAMPLE ANALYSIS REQUEST Stale Laboratory of Publ;c Hcohh lkahh, & Nalural P.:s._--,urrc, 1 · P.O. Box 28047, 306 N. Wilmington Slrt:cl SoJ;d Wa<1c M•nagcmcnl o;,.;s;0n : f) R•lc;gh, No'1h C.roJ;n, 27Gll Si1 e Number ___ "'\ __ -sc,.·' _i~·c~·.s_v)~_-_)--'c 1 .,,_,~;~(~: ,'"-':( ___ ;_;~~/!_JJ"fi; ~ample N umber ___ __,_/.,_!..:;•,,1._-..c·--' _ _-·__,__/ _______ _ Name of Sile _______________ ~_ Site Location L ' ll) ------=--'"'""-"'-''--'------------r / i l/ 2-I Collecled By fr'• v·lt ( I (I~ C " ' ' ; - ( ; ', ' ID,1' /'I /t) Dale Collected Time / ( C,e, I I I I I I I I I I I I I I I ' , , AgcnC)C V Hazardous Waste Solid Waste __ Superfund ------' ' Sample Type ' En"·ironmental Concentrate Comments I ( / Ground water (1) J:f 'I" i,r,,f -hi""& I /l-,,,,,.,-_ Solid (5) -' --Surface waler (2) _ Liquid (6) ' _Soil (3) _ Siudge (7) : Other (4) Other (8) · ' .. ' ~£ ' ~ -'' ---- Organic Chemistry I Inorganic Chemistry Pe ram et er Results(mg/1) Paramder , Results(mg/l)(mg/kg) 1/P&T:GC/MS Arsenic ~· -- . V Acid:B/N Ext. Barium I --MTBE Cadmium· ----Chloride : ----Chromium ----__ Copper ' --Fluoride ----Iron ----Lead ' ---- --__ Manganese --__ Mercury ' --Nitrate I --Selenium 1 --Silver --Radiochemistry --Sulfates ' ······--·---Zinc -- f'aramt-ter Results (PCl/1) _pH __ Gross Alpha --Conductivity Gross Beta TDS ----' TOC ' --' --Microbiology ---- Parumeter Results (Col/!OOml) ' --I ---- ---- Dale Received SEP 2 !l9? eD Reported by Dale Exlraclcdj-9 S,!'3[\, f2C \·•·;;, Dale Reported 8',',1 pr I 7"" ~~'_"•l",;')'i-( \_ ____ ,.l (t ,_., 4, .... ">---·~~ c;.. ' " ' . -r: II _Q ') 1 ~h N11mhrr I TCLP Compounds Inorganic Compound, Results(mg/1) Arsenic --Barium --Cadmium --Chromium --Lead ----Mercury Selenium --Silver -------- -- Organic Compounds Results(mg/1) benzene --carbon tetrachloride --chlordane --chlorobenzene --chloroform --o-cresol --m-ciesol = p-cresol cresol ----1,4-dichlorobenzene 1,2-dichloroethane = 1,1-dichloroelhylene 2,4-dinitrotoluene = heplachlor hexachlorobenzene --hexachlorobutadiene --hexachloroethane --methyl ethyl ketone --nitrobenzene = penlachlorophenol __ pyridine __ telrachloroelhylene __ trichloroethylene __ 2,4,5-trichlorophenol __ 2,4,6-trichlorophenol __ vinyl chloride endrin --lindane --- --mel hoxychlor . _ toxaphene 2,4-D -- --2,4,5-TP (Silvex) -- I I I. '. I STATE LABC«ATOR Of f'VOLIC HEALlH OIVlS [ON oF HE.f-l TH SERVICES. M C. DEPARTMENT OF _HU'1AJI RESCURCES P.O. BOX 280'7 -305 N .. C.[Lr, NGTON, ST., RALE[GH, N.C. 21611 ORCAHIC G<E .[CAL NlALYS!S . \ I I __ PVR_c_cAB__,,L=-E_=_= __ o_s __ .j...!:.!.!'~~.+-_!J:d~'---+JJ~-'-':-.1--t-'-!-"':-"':~'--t----;--;----j-~;--;--+-:--- () ::0, .JC I 'JX I 1-J,.J-::J. I I ) ( ) ( l ( ) I LAB 1-1() c, .:l:)C/.J /r,I q J Jo Y7 FIELD I I ,n_J.C I 11~>;, I I I ( I I I { \ ) ffi".PCUNO lcr-i l orcrrethane rOTOTe thane icMlorodifluororethane vinvl chlorioe hloroethane ethvlene chlorlde l trlchlorofluor~thane ethene 1. 1-dichloro lhane 1 1-dichloro- I, 2-trans-dichloroethene chloroform . · , ·thane 1.2-dichlor6-1-thane 1. 1 1-trichloro- carbontetrachlorlde >rorodi ch loroi-ethane J:--::::oan-e. 1.2-dichloro- 1 . 3-trans--d i ch 1 oro::,rcx,,e~ •-ichlaroethvlen-e .orodibraron?thane .....enzene eth..ane. 1 1.2-trichloro- , 3---: i s--<1 i ch 1 orcorcoene -chlo~thvl vinvl ether l bro-roform ·thane 1. l 2 2-tetrachloro- thene. tetrachloro- I toluene chlarobenzene thv I benzene l a:etone ~utanone arix>ndi ,u I (i de 2--hexanone ...-rethvl-2-oentanone vinvl ace~te TYPE UNITS I,~ n~h I I I I I -v ';;r1-\... '1' I I I I I I I I I I d, I !Oooh I _,; .:., ..... ~ I I I -.v I in..-,,-,h I c.,· ,:,.,h I J:-' I IOppb I I v I .::;~-.h I ' I I I I ¥ I I in--h ~I~ !:5...,,.,h 1n;.,~h I I I •U I I I 'fMDL'f I rUa/ l ..,1Uo/k'o /· uo/ 11 uo/k:o ', I' _... I , I I I I ' I. 1· I. I I, I 'I ,I I ~ rri r .J-.,..,-. ,. ,., I '-' I • I I I I I I I I I I I .. , I ' . , I .J ,--. \,,. ,... -I ~ ,·,. , , . I ; ' I ' I I I ~ ,··,, ,· C I ' I f...\. I ; I ' I I ·, I ' I ' I I ' I I ' I I ' I I ' I .. _, I ·,·v' I I /..l ·, ) " I ' I I I I I I i I I ' I I ' ' I I .I I . I ' I I Estimated value. ( -A:tual value !s Kno.,,n to be less than value give~. Mil \ia/ka uo/ 1 ua/t.'o I ; ' I I I I I I I , I ' J I 1 _ ..... _ I I ! I .1.: -A...tual value· 1s b,own to b-e greater than value given. -t".aterial was ana.lyze-d for but not dete-::te-d. The m.nt>er It'; -Hot analyzed. is the Minim.rn Dete-::tion Limit. ~', -lentative identification. · • -On NRCX: _List of Priority Pol Jut.ants. 1·n.C. n;v; .. ;..,.., -' ti-~, .. L ,.. ____ : __ _ uo/1 ua/'r:o uo/1 uo/k-a I I I I I I I I I I I I I I I I I I I I ii I I I I STATE: LABORATORY Of PUBLIC HEALTH DIVIS 100 Of HEALTH SERVICES, N. C. DEPAAl KENT Of HUH/Ill RESOJRCES P.O. BOX 28047 -306 N. _ll!LM!NGTOO, ST., RALEIGH, N.C. 27611 ' ORGANIC CHEMICAL ANALYSIS BASE/NEUTRAL AND ACID LAB HO EXTRACTABLES FIELD , COtllUJHD TYPE UH!lS .1-n i tros.od irrethv 1 Nni ne /rll:?30 bis(2-ehloroethvl)ether :-ch l orooheno l ,henol l 3-d i ch lorobenzene 1.4-dichlorobenzene .2-dichlorobenzene Ji s (2-eh loroi sooroovl lether hexachloroethane I nltroso-di-n....nroovlamine · ii trobenzene i ,..,._.,.horone '.-ni trnnhenol I 4-dirrethvlohenol bis(2-ehloroethox"'rrethane 2 4-d i ch l orooheno l I 2-4-tri ch l orobenzene .iaohthalene _hexach l orobutadiene .h l oro-m-creso l 1exach l orocvc l ~ntad i ene 2. 4 _ 6-tri ch l oP'VV'>heno l ~-ehloronaohthalene ,cen>nhthvlene dirrethvl □hthalate 2 6-dinitrotoluene 1cenaohthene ~ 4-dinitroohenol SOh&,So 2.4-dinitrotoluene I0l.3.10 I-nitroohenol · ,0/;1-r:o ·1uorene 10/~Eo 4-chloroohenvl □henvlether r 1iethvl ohthalate J, : 6-dinitro-0--eresol So/Jr_,:-,., diohenvlamine /0/330 azobenzene -bronoohenvlohenvlether , ,exach lorobenzene ~ =ntachloroohenol S0//65'0 henanthrene 1,,, r:r:i0 nthracene dibutvl nhthalate .. luoranthene ,~ Estimated value. m1)L H,_o/sotL. •-f._7_,:j J / .. (i_).J.·;-' 7 11.12,·, // __ -,_ -, / ( / 1 ( I l ua/ l :vo/ka ua/ l iJ<>ll<a I,'--I.,.__ ' I I I I I I I I ' I I I I i I I I i ' I I ' : i ' I : ' ' I I ' ! I i : ' ' ' ' : I I i i ' i ' ; I ' : ' I ; I ' I ! I ' ' I I ' i ' ' ' ' I I i I I I I \V \Ji Actual value ls known to be less than value given. -Actual value is kOOW"n to be greater than value given. ·1.].:J·fJ V J /,) _ _)? r / > µa/ l 'unLJcQ -',(__,,. I I I I I I : I : I I I I i I I I : i ; I : ' ; I I I i I i I I I I ' I I I I I ' ' I. \f r l ua/ l ua/ka ( ' ua/1 ua/k□ _ Katerial was analyze<! for but not detecte<I. The nUlt>er I NA -Not analyzed. is the Mininun Detection Limit. m])L --- 1_/ -Tentative identification. _I -On NROC List of Priority Pollutant, .. ( ) ua/1 1JO/ka I I I I I I I I I I I I I I I I I BASE/HEU1RAL ANO ACID EXTRAClABLES COl'IPOUHO pvrene b£nzidine butvl benzvl ohthalate benz(a)anthracene chrvsen-e 3 3-<hchlord:>enzidin-e bis (2-ethvl hexvl lohtha 1 a le di-n-octyl nhthalate ~nzo(b)fluoranthen-e benzo(l:)fluoranlhene benzo(a)pvrene inCY.?no(l .2 3-cd)ovrene dib-enzo(a h)anthracene benzo(o h i l=rvlene aniline ~nzoic acid benzvl alcohol 4-ch l oroan i l i n-e dib-enzofuran 2--<rethvlnaohthalene 2--rrethvl oheno 1 4-<rethvlohenol 2-nitroaniline 3-nitroani 1 lne t-riitroaniline 2 4.5-trichlo~her,ol J - K - l - LI Estimated value. Actual value is known Actual value is ~nown Katerial was analyzed Nol analyzed. STATE LABORA100Y OF PUBLIC HEALlH DIVISION OF HEALTH SERVICES, H.C. OEPAR111EN1 OF HUMH RESOUKCES P.O. BOX 28047 -306 H. WILIIINGlOO, St., RALEIGH, H.C. 21&11 ORGA/l!C ~EIIICAL ANALYSIS LAB 00 '-(. .:;, .:: :, ) (, ..., 7.~''t-' '/ '/,./_,J7 I?' FIELD I I I ;J.-J...; J I t.1. J. I //:l-L:L TYPE r / 'l ( i ) ( ( ) ( ) UH!lS · uol I >w,/ic<J ~ol 1) ,mf-ko u □/ t,l ..a/.-a • ,r,f 1 .. n/ko /0/ ;;:u, -· . I,<.....--i,L--11'-.-- .'>O /Jb'>O ' I /0/.330 I . , I, so//f:,511 Jo/330 ' /O/.J::;,o S"o/,,;, rJ ' ' ,1 ' \y \ ' ' S-0/11-,,c l,LC lfi--j;L. I ' .... / ' /0 /=1'1 I ' I ,:, ' 5'o/J"5o ' \I/ \ ' ' \ I ' ' ' ' ' ' m1H-, H:z.OI Soft,;. to be less than value :given. to be greater than value given. for but not detected. lhe nurber is the ~inirrun Detection Limit. HA - 1/ 2/ - lentative identification. On NROC List of Priority Pollutants. r l ( 1 ,1n/ 1 un/k"Q un/ 1 un/1:Q --- I I I I I I I I I I I I --;:;~ /•' ,, ~ ,7~ /-'.'.:.. ·.-.l-~ -:-._~'\ !_.,, -·,,,\ ~; --. \ (:; ::n um <,\ State of North Grolina .~. R;,;ei,,,, ' \1 Department of Environment, Health, and N~~f"R~µtces Mooresville Regional Office '(,,. ' ·-,~~_:, ·. ' Jam.ea B. Bunt, Jr., Governor Jonathan B. Bowea, Secretary DIVISION OF ENVIRONMENTAL MANAGEMENT Mr. Mumford Route 14, Box 357 Statesville, North Dear Mr. Mumford: May 19, 1993 ' Carolina 28677 S~bject: ' On February 22, 1993, :I sampled your well for nitrate/nitrite, metals, total dissolved solids, coliform, and volatile organic compounds.: The results indicate that nitrates and nitrites are present at levels (13 mg/1) just above the 10 mg/1 groundwater standard. The level found should not be harmful to adults, however, children under one year of age should not drink it. ' Merc_ury was also present in the well at . 0016 mg/1 which is ,·u~r hPlo~ thP ~p• dr"nk1.'n~1 w~~~-~t--~--a -~ 002 =-/1 _ ~----• ,..,------~ --• • ~ .,_._.,_.._ -, a,J.'-"O.L VL • ill~ • Manganese was present at .066 mg/1 which is above the secondary drinking water standard of .050. The level present should not pose a health risk, but may 1 cause staining of fixtures or laundry. : The remainder of metals and organic chemicals that were found were below both North ',Carolina's groundwater 'standards and the EPA drinking water standards. ' We will continue to monitor the well for mercury and nitrate. PO. Ila< 950, 919 North Main Sattt. Moo«<Vlllc, NC lBIIS-0950 • Telephone 704,663-1699 • FAX 704,663,{l)4() ' An E,;ill21 Oppanunity AffinnariV< kt',o,n Emplc,y<r I I I I I I I I I I I I I I I I I -- 1 I Mr. Mumford ·May 19, 1993 Page Two· ' If you have any questions, please call me at (704) 663-1699, ext. 235. Sin4 :e~y, :~~ Chris DeRoller Hydrogeologist ' cc: Iredell County Health Department Laurie Martin, Hazardous Waste Section Julian Foscue, Solid Waste Section CMD/sc ------------------- ' cour, r, J, rl li• // OUAD No.l.//7,1·~/ SEJllAL NO. ___ _ North··Carolina LAB NUMBER 8 :\C--::rci'zs() Doparlrnont ol Envrronrnonl, Health, and Natural Resources 2,,6 3 0~ q ·uc) Division ol Environmental Management DATE REc~D= 1,_ T~~- Groundwalor Fiold/Lab Form Rec'd by: :=, From: au,~ neporl lo: wano. wrno. 1:.\ ~\~! fl;t f'H'~'~°{j;'K\J •;; ' > ,,H. SAMPLE-'pffiO'BJ:t~~ I 0 Olher -------------.-,--- c K £.1,1t /(/ DATA ENTRY BY: _ _,.,.L)..L/,._{ __ WSRO, Klnslon FO Olhor ________ _ □ ROUTINE ~ EMERGENCY DATE n EPO n TED: ~3:...lu.l_rl,.c/...:1-':...' ------Slltpped by: Ou~ Olhor ______ _ /T-77 /. COLLECTOll[S): fl(/,~ r...C FIELD ANALYSES D11 400 ____ Spoc. Cond.114 ___ 012s0c Tornp.10 ____ ·oc Odor _______ _ Apponronco ----~--Tes10 ______ _ Field Analysts Dy: ___________ _ L/\IJOll/\lOllY /\N/\LYSES nou6 Jlo melt x COO ltlgh HO mg/I COO Lo,. '" mg/I ><' Colllo1m:ur F ■CII J!616 .L_/ J:IIOOml Colllorm:ur Tot■I J 150◄ /lOOml Toe 6110 fllg/1 lurbldllr 16 HTU pit 4 OJ unit■ At~ •11nl1J lo pll ( ,!) 410 mg/I A lit ■llnlly lo pit 11,J ◄ U mg/I Cubo<Uh ... ma/I Blcubon111 ... mg/I ArunJc:Tolll 1002 UOII C11bon dlo•ld• ◄0!) mg/I 'y Chlruld• 1140 mg/I ChrumlU<O:lh ■ IOH ug/1 Coh,r:Tn,.. 110 Pl·Co cr•nld• "" mg/I lab Cornrnenls: -_I -C /74.,1~--- PURPOSE: 0ASELINE, COMPLAINT, COMPLIANCE, LUST, OTHER _____ _ (clrch ,one) Ow nor /'( l oc a I I on or s I Io --'-'-'.:.<_.,:-'.:;>-.:;1,.c·•c..G,.,__·_.1_· _ _;fJi:-~:_;lc.· "'"h'---"5-'· •.:.•·.o'..c'·~/c...::<_,' u«-,:,Y_· -'-''-''rc_lc._:•.:.'f-s:'c..':..r,:1 __ 1c-'-''<:..'..:~:..· ,:'°:..''_· _..:S:;,,,::0_•;_, ,;,r(_,,_;.0;_/ __ r_c,_,._;,/~.e.. Ooscrlollon ol sompllng polnl ,,·(/ Sampllnn Method ---_____ _,c:-J:....,.,(_·lc.-_· -1/Jc:..,,1..i{.,'t:...>CJ.l.,i•"'"--------S amp I e lnlerve I ____________ _ (pump, boiler, loicJ I nomarks c.,.! (( J;',-, ,. ,·.fr,,·/ 1F 3<[ Z ''?__ ,Olc1c1 se ,u, ,,;1 '(Jn-1,?(.,IJ ,, o I· Din. Solld1 10JOO IJ-0 mc/1 rluorld• 851 mgll H11dn111:To111 ,oo mg/I J-h rdn• 11 {non-cub J "' mg/I P/1tnol I Jl 1 JO uofl Spu::lllc Cond. " uMho■/cm 1 Sull111 9 ◄5 mg/I S11llld1 7 ◄ S mg// HIIJ I I ~j Ii 10 o. o·) m11tl TKN .. " 0" mg/I N02 1 PIOJ II N ,,. ,·~. mg/I P:l oT■I II P 66S mg/I (pumPlrl'J ltme, air lomp, elc.l Ci,, /c., /7 ::> / I' fSr<v·(c; ( 1 /~A I ( ·c, it' /7.:.>f J>_,,,f'Y<rv ,, • 511 vu 10n ug/1 01gll'IOChlorlnt f1,1lcld1t Al -Alumlnum 1105 -<"S(; ug/1 01111nopho1phoru1 P11lloldt1 ,Y 81 -Bui um ·1001 ~,.., ,•ft') Ug/1 >( c, • C ■lclum "' .vf-c, ~ I mg/I Acid Httdloldtl >< Cd • C ■dmlum I 021 . 2--f ( ~✓ r;,u1111 >< Chromlum:Tol■I lOJ ◄ <:.·{~) Ug/1 e,u / H,u1r,1 E•lt1cllbl1 0111•"111 X Cu • Copp., 10◄2 :l? ug/1 Acid Eilr1cl1blt Qrg11,lo1 >< ,, • Iron 1045 I i~O ug/1 )( lig -Mucury r 11100 I, (n UII II v Purgubl• oro1nlc1 (VOA bolll■J >' K -Poll11lum gJ7 .1,X-mg/I . -Mg -k,hgn■■lum 921 --r-. 5 moJI 1,1 • Olbromo;lhlnl IEOel V Mn -),hng1n1u 1056 :~.( .. UQ/1 >< th -Sodium 11211 ',, 3 mgtl ;,,' '" • HI ck I I 1061 < /() ug/1 ; v' rb -LI Id IO S I ✓-I(;) ug/1 s, S■l,nlum I 147 ug II ' I L l" . Zinc ,o,~'P,.-·1JllPI-...ru, ·"" I/ , . .liliSOUJtCES ,.., '-'"-1 l J. I IJEYE!.QJ• IF ·,r '"R ...... 2 5 l;'Y.5 . ·-,--- I,,. I ! LAB NO. JG280 P.EPOP.TED BY ~ I CHECT.ED BY ' /(Xf'__ REVIE'iED BY a#« 1, SAMPLE TYPE: 'iATER CASI VOA TARGET COMPOUND TQL I ua/1 15-35-1 1,1-Dichloroethene 0.15 15-09-2 Methylene Chloride 0.25 IC li&-6D-5 trans-1,2-Dichloroethene 0. l 5 15-Jl·l l,l·Dichloroethane 0.25 590-20-7 2,2-Dichloropropane 0.25 I m-59-4 cis-1,2-Dichloroethene 0.25 07-66-3 Chloroform 0.25 H-57·5 Broaochlorouethane 0.15 11-55-6 l, l , l ·Trichloroethane 0.25 I 56l·i8·6 l,l·Dichloropropene D.25 •. 56-23-5 carbon Tetrachloride 0.15 101-06-2 1,2-Dichloroethane 0.25 I 75-01·6 !rich] oroe thene 0.25 76-81-5 1,2-Dichloropropane 0. 25 li-21-4 Bromodichloroaethane 0.25 I H-95·3 Dihrouoaethane l i006i·Ol·5 cis-1,J-Dichloropropene 0, 25 !0061-02·6 trans-1,l·Dichloropropene 0. 2 5 I 19-00-5 1,1,2-Trichloroethane 0.25 111-18-4 Tetrachloroethene 0.25 ll2·28·9 l,l·Dichloropropane 0. 2 5 121·!8·1 Dibroaochloroaethane 0.75 I 106-93·! 1,2-Dibroaoethane l 108-90-7 Chlorobenzene 0. 25 630-20-6 1,1,1,2-Tetrachloroethane D.25 I 75-25-2 Broaoform 0. 5 19-34-5 1,1,2,2-Tetrachloroethane 0.15 I TQL· Target Quantitation Liait· Subject to change due to instruuent sensitivity T· Tentatively Identified, not confiraed I E· Estiaated value U· Samples analyzed for this coupound but not detected I N· Sauple not analyzed for this coapound D· Detected helow quantitation liait M· GC/MS Analysis perforaed I CO!!.'!ENTS: I ii I EHNR/DEX LABORATORY VOLATILE AHALYTICAL REPORT SurEiiVISOR ~ DATE ~ 3 ENTERED BY • CiilCKED EY Ynt.£-/ ANALYSIS RESULTS DETECTED uo 1 D D D D u u u u u u u u u u u u u u u u u u u u u u u CASI VOA TARGET COMPOUND 96-18·4 i,2,3-Trichloropropane 108-86-1 Bromobenzene 95-49·8 2-Chl orotol uene 106·!3·4 4-Chlorotoluene 541-73·1 1,3-Dichlorobenzene 106-46-7 1,4-Dichlorobenzene 95-50·1 1,2-Dichiorobenzene 96-12-8 1,2-Dibromo-3-Chloropropane 120-82·1 1,2,4-Trichlorobenzene 81-68·3 Hexachlorobutadiene 81-61-6 1,2,3-Trichlorobenzene 1634-04-4 Hethyl-tert-hutyl ether 71-43·2 Benzene 108-BB-3 Toluene 100·!1·! Ethyl benzene 108-38·3 .,p-Xylenes 95-47·6 a-Xylene 100-42-5 styrene 98-82·8 !sopropylbenzene 103-65-1 n-Propylbenzene 108-61-8 l,3,i·7rimethylbenzene 98-06-6 tert-Butylhenzene 95-63-6 1,2,4-Triaethylbenzene 135-98·8 sec-Butylbenzene 99-81-6 p-isopropyitoluene 104-51·8 n-Butylbenzene 91-20-J Naphthalene Other purqeallles detected (up to JO highest peaks) HO VOL~T!LE ORTGAliIC COMPOUIIDS QUAHTITATED BY GC/PID. 7QL ua/1 0.25 1 0.25 0.25 0.25 0.25 D.25 1 0. 25 0.25 O,i5 D!i3CT:: uc!! Dete::,d ug/i ----- - -, . ---- - ---- - - GROUNDWATER FIELD/LAB FORM . North Carolina , >f._ I'.•/ ... L ,·), {~~' D.fPi\';\ri\.!ir;il(p(l~hvl(onmenl, Heallh, end Nalural Resources •Lnu -~, ~"□1w1r:JN 05'!;N'l!FldNMENTAL MANAGEMENT. GROUNDWATER sEcnoN Counly_~=~---------- Ouad No L([)111-!, 1 Serial No. _____ _ Lal. ,35° '.J a/ 5 6 ,, Long. ~'&~0~0~5~8_'~1_4~'-' __ SAMPLE PRIORITY Report To: ARO, FRO, ~RAO, WaRO, WiRO, WSRO, Kinslon FO, Fod. Trusl, Cenlral 011., Other: ________ _ □ROUTINE 0EMERGENCY [ZjCHAIN OF CUSTODY 0 Shipped by: Bus, ~Hand Del., O\her_· ___________ _ ~ Purpose: . Colloclor(s): tUua f k:µ Dale 3 ·_ la .q5" Time I 2 : ':IS: ah Baseline, Complain!, Compliance, LUST, Peslicide Sludy, Federal Trust, Other: Poll uh'"" 11"": F""J I" C I 1cHI• ooa) EIELD ANALYSES Owner A II l. r. a.sco..c Jo,-, Gw 1~<-" 1,31. -s . .,..,Gn' al 25° c Location or sile .1;'.o<,,.b:. l'I &ck 3s '1 ShJ-e,;u i I I" f'\J<. z.. 9 "''l '7 Descriplion of sampling poinl Is, kh <o :s ·, ~ k.. 'Sf' '{)O± Sampling Melhod _f~l,\._rl.~l"----~==~~-------Sample Interval _______ _ c t:; (Purrv baii.,, ••ci Remarks ,_;,a,...p I, c\ a.! -+-e., :f u.M.f ·, ,:..'!> "' '5 M; n .s (p,Jmp...g bm•. 10" ltlf'4l. etc.) pH400 (o, o Spec. Cond.,. ,,---- Temp.10 .,.----0 c Odor _ru===---- Appearance _.._cR,_,ll,,.0/y"-"'------------ Fiold Analysis By: L}'v-"-W=u.,J.--"1@-=. _______ _ LABORATORY ANALYSES BOD, 310 mg,1 Diss. Solids 70300 mg/I Ag • Silver 46566 UcVI Organochlorine Peslicides COD High 340 mg/I Flouride 951 rmvl Al • Aluminum 46557 uo,I Orgaoophosphorus Pesticides COD Low 335 mqtl !:facdness; To!al 900 rn!l'l. As• Arsenic 46551 uq/1 Nitrogen Pesticides Coliform: MF Fecal 31616 /100ml Hardness {non-carb) 902 mg/I Ba • Barium 46558 ua/1 Coliform: MF Tola! 31504 1100ml f'J1eno/,; 32730 ua/1 Ca · Calcium 46552 111(jll Acid Herbicidos TOC 680 mq/1 Specilic Cond, 95 uMh□s/cm2 Cd • Cadmium 46559 uqtl -- Tutbidily 76 NTU Sulfate 945 m<lil Cr • Chromium 46560 ua/1 Semivolatile Organics Residue., Susp.ondod 530 mgll Sullido 745 m(J/1 . Cu · Coeeor 46562 ugtl Fe• Iron -46563 ugll X Hg • Morcury 71900 L, L ugil ~ Volalilll Organics (VOA bottle) ' pH ◄OJ unit: K • Potassium -46555 mgtl Alkalinity lo pH 4.5 410 mgll Mg • Magnesium 46554 mq.l TPH -Gasoline Range Alkalinily lo pH 8.3 415 mg/I Mn• Manganese 46565 ua/1 TPH . BTEX Gasoline Range Carbonale ◄45 , mg/I NH. asNs1o0,01 mq/1 Na -Sodium 46556 .. . fTl!l'I N.C. 0 c::r;-T~t:'. r .T' Bicarbonate 440 . mq.11 .Ilili..as1Lfi2' --mg/I_ N;. N;rkel un/1 E,NVII\.Vl .. A 1' l;.;;c:.llllllCF' Carbon dioxide 405 · ma/I X NOR + NO, as N 630 /b, mg/I Pb· Load 46564 ua/1 QI •.• -• Chloride 940 mgll P: Total as P 665 mo/I Se • Selenium ug,1 , • ......... 'I O \qqc; -I ... Chromium: Hex 1032 ug,1 Zn--Zinc 46567 ua/1 \ Color: True so Pt-Co \/ . HltW Cyanide 720 mgtl . !IVIS:Ctt Of. lHVIROn"'""" ''.~'"' nl . ~DU,n.;i .. ~~~ ---- Lab Comments:---------------------------------------------------------- GW-54 f1EV. For Dissolved Analysis • submit filtered samplo anU wri!o ~DIS" in h -- --.... .. - - REPORTED BY ~ CHECKED BY REVIEWED BY SAMPLE TYPE: WATER 75-35-4 1, 1-Dichloroethene 0.75 75-09-2 Methylene Chloride 10 156-60-5 trans-1,2-0ichloroethene 0.75 75-34-3 1, 1-Dichloroethane 0.25 590-20-7 2, 2-Dichloropropane 0.25 156-59-4 cis-1,2-Dichloroethene 0.25 67-66-3 Chloroform 0.25 74-97-5 Bromocl1foromethane 0.75 71-55-6 1, 1, 1-Trichloroethane 0.25 563-58-6 1, 1-Dichloropropene 0.25 56-23-5 Carbon Tetrachlodde 0.75 107-06-2 1,2-Dichloroethane 0.25 79-01-6 Trichloroethene 0.25 78-87-5 1,2-0ichloropropano 0.25 75-27-4 Bromodichfororne I ha ne 0.25 74.95.3 Dibrornornethane 1 10061-01-5 cis-1, 3-0ichloropropene 0.25 10061-02-6 t.rans-1,3-Dichloropropeno 0.25 79-00-5 1, 1, 2-Trichloroethane 0.25 127-18-4 T etr achloroethene 0.25 142-28-9 1,3-Dichforopropane 0.25 124-48-1 Dibron10chloromethane 0. 75 106-93-4 1,2-Dibromoethane 108-90-7 Chlorobemene 0.25 630-20-6 1, 1, 1,2-Tetrachloroethane 0.25 75-25-2 Bromoform 0.5 79.34.5 1, 1,2.2-Tetrachloroethane 0.75 TOL-Target Quantitation Limit· Subject to change due lo instrument sensitivity T-Tentatively Identified, not confirmed E-Estimated Value U-Samples analyzed for this compound but not detected N-Sample not analyzed ror this compound D-Detected below quantitalion limit M-GC/MS Analysis perform.ed COM~ ·s: --- -EHNR/Dt::M LABORATORY VOLATILE ANALYTICAL REPORT ANALYSIS RES UL TS u 96-1 8-4 1,2,3-Trichloropropane u 108-86-1 Bromobenzene u 95-49-8 2-Chlorotofuene 1.5 106-43-4 4-Chlorotoluene u 541-73-1 1,3-Dichlorobenzene 3.5 106-46-7 1,4-Dichlorobenzene DT 95-50-1 1,2-Dichlorobenzene u 96-12-8 1,2-Dibromo-3-Chloropropane u 120-82-1 1,2,4-Trichlorobenzene u 87-68-3 Ho x achlorobut adiene u 87 61-6 1, 2, 3-T richlorobenzene u 1634-04-4 Methyl-tart-butyl ether D 71-43-2 Benzene u 1 08-88-3 Toluene u 100-41-4 Ethyl benzene u 1 08-38-3 rn,p-Xytcnes u 95-47-6 a-Xylene u 100-42-5 Styrene u 98-82-8 lsopropylbenzene u 103-65-1 n-Propylbenzene u 108-67-8 1,3,5-Trimethylbenzene u 98-06-6 tert-Butylbenzene u 95-63-6 1,2,4-Trimethylbenzene u 135-98-8 sec-Butylbemene u 99-87-6 p-isopropy Jt oluene u 104-51-8 n-Butylbenzene u 91-20-3 Naphthaleno Other purgeables detected (up to 1 0 highest peaks) ONE UNIDENTIFIED PEAK DETECTED BY GC/ELCD. ONE UNIDENTIFIED PEAK DETECTED BY GC/PID. LAB NO. 6G307 SUPERVISOR DATE ENTERED BY CHECKED BY 0.25 0.25 0.25 0.25 0,25 0.25 0.25 0.25 0.75 5 2 0.27 Detected ug/L u u u u u u u u u u u u u u u u u u u u u u u u u u I I I I I I I I I I I I I I DEHNR MOORESVILLE R 0 State of North Carolina Deportment of Environment, Health and Natural Resources Division of Water Quality James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary A. Preston Howard, Jr., P.E .. Director Dec 5 '96 12=54 DIVISION OF WATER QUALITY November 20, 1996 Mike James 177 Lauren Drive Statesville, North Carolina 28677 Dear Mr. James: RE: Health Risk Evaluation James Well Iredell County P.06 l have enclosed the health risk evaluation for the water sample taken from your well on September 5, 1996. l received your phone call, but your phone number was lost when my computer crashed, so I could not return your call, If you have any questions, please call me at (704) 663-1699, ext. 234, lnclosures rd\j:l..,.•.hr1 P.O. Box 29535, Roieigh. North Carolina 27626-05.35 Telephone 919-733-7015 Sincerely, ~0~--- Paul R. Dahlen, P.G. Hydrogeologist FAX 919-733-2496 An Equal Oppc,rtvni1y/Affirrnative Action Errployer 5aX, recyeles/lITT, post-consumer paper I I I I . 1 I I I I I I I I I I I I I DEHNR MOORESVILLE R 0 Dec 5 '96 12:54 P.07 North Carolina Department of Environment, Health, and Natural Resources Division of Epidemiology Occupational and Environmental Epidemiology Section Medical Evaluation and Risk Assessment Branch Drinking Water Health Risk Evaluation . General --£4 County DAT~_~fl ..... )3_)1_6 __ LABORATORY NUMBER ---"{~&_·~)1_/_0 ___ _ ( ) Based on these analytical results. this water should be considered safe for normal usage . ( ) (X) () ( ) (X) Chemical analysis did not show any contilmination. Water should be resampled if odor or taste persists. The Willer should not be used for drinking or cooking purposes. Bilsed on these analytical results, this water is highly contaminated and should not be used for drinking, cooking, or bathlng/showertng. The laboratory results are not conclusive. pl..ase resample. PLEASE INDICATE ON LAB SHEET THAT IT IS A RESAMPLE AND PROVIDE PREVIOUS SAMPLES NUMBERCS/ COMMENTS: The nitrate drinking water standard is 1 o ppm. The nitrate level in your well water is either above or close to the drinking water standard. Continued consumption, csoeciallv for pregnant women or infants six months of age and younger may pose an increased health risk based on these nitrate levels For further information. contact Dr. Ken Rudo. Occupational and Environmenral Epidemiology Section. (919) 715-6430. DEHNR 3891 (1/96) Occupational and Environmental Epidemiology Section (Review 1/97) ------ :P-OR I TO MRO lt.qj:,DMI O!fo« Jt.LECTO~S> -iof,~l~IL~tN;c;,------- ,TE. ~ "' J!lf'OSL:· 1\BORATORY ANALYSIS l!oU JIil COU llil,h )40 (:OD l,,,,, lJJ Cahf..-m: MFTotal) 1»4 JIOOroil roc "'" I! w,iu Alblini.(y topll ll ..... lk•b<,,14[,e {:w,bon.dio:>i=.:k <.hJ...,,,uk ..,,,_ »HIENlS: L.c:Slill'l'l.,. Sec ~i~ cf 1,1,111plinii poi• S--v!ina. Mc-hod· ._ .. Ow. Soltdl lDJOO fl_.iJc~I I laod't.-u._ 1..ul 9CO I b,,,!na,... t....n-cllilJ 902 Ph.rnc,l1J27JO S~if.c CQ114 '9!1 Sul1.-.c, SuUidr 145 MOMi O,l.-ldCJrnx: S.,1,u ·~~ t,itU ..,.t,l,(,,10 TKt-lnJU.H X NU:? iNOJni,ft.10 r ·ru1~1;Hrt>(>5 ro-• ------- 111n~ION Ur t:NVIKllNMENJ"AI. ~IANAGEMENT Oin.lS.lry L..l.enllM')' Arr-1 JC.-.~•• Wu,.. v-,1~-• \' J ! • · .::· I" f. } 1 SAMM,.E ERtoklIY O•oun"" IBJEMElGENCY ti NA'l'UH.,\l~ Rr· OCl 25 1996' ... .) g] ('Jltl.lNOFCUSl0OY El SAM KE TY PE □ .'.:; '-~~~i~f! rn l,,ALIRN Ui\ sun:s\1 l.LE Ll.iL\:~t! .;, ... ia ,1,.cr m.L .l.g-Scl~cr «SM ,.,._ mrL .U-Aklfflinua tb5~1 ,.,._ m,C .h-ArW'nM:'6-S$1 ,.,._ ... L UJ--B.11WT1 «i-S ~B ,.,,_ u11:•l ra-Cakilll11•Mn ..,,_ u~ lhoi/rn,.? CH..Jw.fT!t6l5'l' ".,._ m,'\. C,-Chrorni,m ¼S60 ,.,,_ mi,'l Co-•C"1>9J'C"IOU: ,_L rn'll'I, f,e,-J,.,.. Jc»5 ".,._ ri1!S'I, ' 111!--Mcn:ury 11900 I ' 1.J ""' rn11·L i;,.r«;U:Siu.n .;t,5,s .... /\Ii· /\1q.nu,11m Q,21 -/\ln-l\1=-11!:.r'l'e~ 10~, •o'L 0.0-< ~•L Na.-Sodiun !)lQ ""'L myL ~t-N1d,d ~IVL " 11riv1. l'b·l..tJJJ--t<>i6-t ...,._ ,nrl. Sc-!'iclt"-IUJI . .,,_ '"'11'1, 1. ... z,nc -tc.s.c.1 ..... ---- ........... ' 6GlYIIO 0-Jtoeei•ad: ..,,...,.. firt>e lhoti'<OI 12:00 AM ......,..,. ttMW ~By: OS Du;q,c:,rtcd: lCVll,".16 a.~~ --t,l~~ Acid Ue.bocidu • Tft~~ X v.-k Otpni.::1 l VOA bcd,,:ct Il'll-<na>li.c ~ lPIL-DTEXG~i"'l" R~, II01tN ..... - t::J fTl I z "' 8 f?i (/) C >-< r r;:; "' D t::J (1) n Vl "'C) 0 00 - - REPORTED BY CHECKEDBY REV1E-DBY SAMPLE TYPE: 75-35-< 75-0G-2 156-00-5 75-3-4-3 590-20-7 156-~9-<4 67-66-3 74-97-5 71-~-6 663-M-8 se-n-5 107-00-2 fQ-..(Jt-6 UHJ7-5 75-27-4 7.4-4;!5,..3 10061-0t-5 10061-02-6 7~ 127-IM 1◄2-28-9 12.$--48--1 100-93 ◄ 108-00-7 630-,o.;3 75-25--2 79-!4-S -- WATER l, 1-Oidiloroethene Melhy1«N Chloridil lre.ni,-1,2-0K;hlof~lhene I, 1 ·Dlchklroe\hane 2, 2-0k:h1Nop<opall8 c.15-1.2-0t:hkm:lEllhen& ChkJrofcwm 9romodll:xomeltr.1M 1.l,1-Tr~ 1. 1-~ne Certxx. Talradiloroe 1,2-DichloroelhGne T ncNorotlhet\e I .2-Dlchk,ropropane S.omodidlk>fomeltlartie Dibrnnt.ome1he ne 0$--1, 3-0chloropropene lran:s-1,3-0il::hlol'QllfOP&MI 1. 1 .2-T nchloroo°""" T •-,.~ D ibl ~ \ .2-Dibc~ham Chkxooeozone \, t, ~.2-T~lhane B!omolooTI 1, 1,2,2-Tebachloroett1soe lQl-Tergel Quanlllalio"I limit-Sutjed. kl ctuirve <l\Jl!I to imnnnent smsilivity T-Tl!llntM!iYefy ktcn.6fied, no( OJnl'irmed E-Estimated vuue -! - 0.75 10 0.75 D.2S 0.25 0.25 0.25 0.75 0.25 0.25 0.75 o.z~ 0.2:S 0.25 0.2:S 1 0.25 IJ.25 0.25 0.25 0.25 0.75 1 0.25 0.25 o.s 0.7S lJ.-Samp!e• a.nolyzed fcf lhio wm,,ound bul ""' detected K-. S.mplo nol onal-/md fo< this OOOlpOIJnd D-Detected bvlow q,.i•nma1iorl limLI. r.t. GCJMS Analysis r,,<bnN,d ---EHNR/DEM LABOR.ATOR'Y VOL.411LE ANALYTtCAL REPORT ANAL TSIS RES UL T5 u %-1!!-4 u 108·65-I u 95-49-6 1.2 IOE-43--11 u 541-73-t J.◄ ET 10E .... 6-7 u 95-50-1 -- 1.2.3--T richloro propane 8 rornotenzene 2-C hlorntotue ne ◄· Chlorolotvene \.J-~ene 1,4-Dichkxobenu1nit 1.2-Dlchloroberuena --. ._ _J --LAB f.tO. t01NO SUPERVISOR~ OAlE~ ENTEREDB DME V 0.25 u t u 0.25 u 0.25 u 0.25 u 0.25 D 0.25 u u .. %-t2-8 \ ,2 · Ditxomo-J.Otlof op« or,zme ' u u 1Zo--62·1 t ,2,-4-liid 1lo.obe1lLeno& 0.25 u u P.7-68-3 H~eoene 0.25 u u 87-6~-6 1, 2, 3-focN::.robenz ene, . 0.75 u 0.5'3 163~-04 ..... Me\.hyHa.-l·buttl ethef" s u u 71-43--2 S,nu,re 1 u u 10H6-3 Toluer<> u u JCX)--41-4 Elhyl benzer-.e-1 u u 1011-38-3 m,p--Xv'.snes 2 u u 95-47-0 o-Xylere u u 100.;42-$ s.,,,..., u u eH.2-8 ls<,j)ro<lyllenzeno u u 103-SS-t n-P,opilbenz:e ne u u 1~-87~ 1,3, 5-1 rmetl))l lben.Ze-fle u u 9!-06-6 ~-Bu1~ u u 95--63--6 1,2,-4-Tlimislhytben.zene u u 1JS-9H s.ec-Butytberu:ene-u u 99--1!17-E p-~yll!otuaoo ' u u 10+-51-S n-Butylben.zeoe 1 u u 91-20-J Naphthalene I u IGuol;ne a .. .,.,. E,1;mated T011" Peuol<!um HJdn,aart>a, I moit mg/l ·I 0.25 Olher pur-vMbtes del&ct&d De- \up lo 10 h;ghesl l)l}aks) '-9'1. MO VOi.A TILE ORG,P,.N,IC COMPOUNDS OElEClED B'f GC/PlD. COfdMENTS: SAMPLE ut,IREFRIGER.ATEO DUE lO HURRICANE FRAN. -~~==-======-=--'-"--'-====-="'--------------------------------- --- 16' n (.fl \.0 ry, :-u 0 \.0 1. I I I I I I I I I I I I I I I I State of North Carolina Department of Environment, Health and Natural Resources Mooresville Regional Office James B. Hunt. Jr., Governor Jonathan B. Howes, Secretary DIVISION OF WATER QUALITY May 28, 1997 Mike James 177 Lauren Drive Statesville, North Carolina 28677 Dear Mr. James: RE: Health Risk Evaluation James Well Iredell County I have enclosed the health risk evaluation for the water sample taken from your well on April 8, 1997. I will be resampling this well in July. If you have any questions, please call me at (704) 663-1699, ext. 234. ) closures : Allen rd\james.hrl Cascaddan 919 North Main Street. Mooresville, North Carolina 28115 Voice 704-663-1699 Sincerely, ~\ol--- Paul R. Dahlen, P.G. Hydrogeologist FAX 704-663-6040 j-8:§ Li.. J ?fr##':i An Equal Opportunity/ Affirmative Action Employer 50",{, recycled/10"/o post-consumer paper I I I I I I. I I I I I I I I I I I I I () ( ) (X) ( ) ( ) (X) North Carolina Department of Environment, Health, and Natural Resources Division of Epidemiology Occupational and Environmental Epidemiology Section Medical Evaluation and Risk Assessment Branch MAY 28 i ~y DATE_.:::...5,-'-/~_)...1.../-'--1J-"------LABORATORY NUMBER ___ ;--"-"'f-_0_1_:_f'__:_) __ _ Based on these analytical results, this water should be considered safe for normal usage. Chemical analysis did not show any contamination. Water should be resampled if odor or taste persists. The water should not be used for drinking or cooking purposes. Based on these analytical results, this water is highly contaminated and should not be used for drinking, cooking, or bathing/showering. The laboratory results are not conclusive, please resample. PLEASE IND/CA TE ON LAB SHEET THAT IT IS A RESAMPLE AND PROV/flE PREVIOUS SAMPLES NUMBER(S) COMMENTS: The nitrate drinking water standard is 1 O oom. The nitrate level in vour well water is either above or close to the drinkina water standard. Continued consumotion, esoecially for oregnant women or infants six months of aae and younoer may pose an increased health risk based on these nitrate levels 04 J, For further information, contact Dr. Ken Rudo, Occupational and Environmental Epidemiology Section, (919) 715-6430. DEHNR 3891 (1/96) Occupational and Environmental Epidemiology Section (Review 1/97) - COUNTY QUAD NO: - IIIEDELL - - ---- - - Dl\'ISION OF WATEH QUALITY Chrmi,lt") I.Al,or11for1 llrpo,t I f:10111111 \\'Aln l)uAlil) SAMPLE rRIQRI TY E)Rot!I INE □Et,.11:R(if:NCY RHORTTO COLLECTOR(S) UAlE; _,_,_R_O _________ Regional Office (D Cll,\IN Or: CUSTODY E] 5At,.1PLE TYPE □ DAIii.EN TIIIII:: rlJRl'OSE: LABORATOllY ANALYSIS uon J10 rug/L COO lligh J-10 mg/L COO LowJn rng!L Coliform: MF Fcc.11 J 1616 1100ml Colifonn: MF Total Jl SO-I 1100ml lOC mg/I luibi1i1y NIU Residue . Suspended SlO mg!L I 01at Suspended solids mg!L ,11 ,11,i1, Alkalini1y lo pll 4.5 mg/L A1lalinil>' lo pll 8.J mg!L C11rl>onale n,glL Bica,bonatc mg/L C111l>on dio~idc 1111!/I. Chlu1idc 1111111. Ch,omium I le.~ 1032 "!!-IL Coloi: True 80 c.u. Cyanide 720 "'1:\/L CO,\IMENTS: l.oc:i.tion or Site; Oese1ip1ion of sampling point Sampling Mclhod: Rcm,uks Ilia, Solid, 701(1(1 l'luolide 951 I lardncss. total 900 I lardness: (non•carbl 902 l'henols 32730 Specific Cond. 95 Sulfo1c Sulfide HS l\111AS Oil and ti,casc SilicP lloron rorm11hleh1 de NIO os N 610 rKN as N 6n -' NU2 +NOJ a1 n (JJO I'. ·1n1al ~s I' (J(,S 1'04 CJ,!..EN L\SC'AIJJ(t:.Ii n•ic-11. mglL Al-,\luminum 46557 mg/I. mg!L lla-llariu,11 4GS58 uglL Ca-Calcium 4655~ ul\lho,/cm2 Cd-Cadium 46559 mg/I. r,.Cluumiu,n 46560 u,i;fL Cu-Cuppcr IOI~ m;:/L Fe-hon 1045 mg/I. ,ngll. mgll, 0.01 mglL mgll Ni-Nici.el 12 n,i;/1. <0.01 mi;H. Sc-Sclcniurn "'!!-'L /11_ I.inc 4h5h7 - - --N.C. Dhr'T. CW tr,N,V!HOn~f~N'f, 11£.-'L'IS.H. {J Nr\TlittAI. RE30lll{CES MAY 14 1997 DIVISIO! Uf [¥11.BIU!U[illl wmu~ T ,;.y:StHlH l!llil11!l !ITIC£ - l.nh Numhc, n:uc Rccci,cJ Time Rccciscd Rccci,cd ll)· Rdc.iscJ th 0JIC 1cportcd; ll1~:111uchlori11c l'cs1icidcs rngl\, ,\cid I lc,biciJcs Scmi,olalilcs 11'11-\licscl R;msc ug/1. - - - 7(;1m11 -llll197 CJOOMd ns l>S 511)197 IG018 I ~PA ,.. --- --.. -_J]IIIIIIIII - ---... -·····---------I· o I I. GROUI. -WATER FIELD/LAB FORM Ocpntltncml of Envlronrnc>nl, llcnll/1, rnld flalurn/ ncsourcc9·· ' ' I\ ) . JJIVISIOII OF EtlVlnOlll,IEIIT /IL M/111/IGEMEIH • GnOUIIDW/1 TEn SECTIOll County ku.L Ji Quad No l/,7 n '1 Serial No. ______ _ . -~ ' neporl To: Ano. rno.~nno, Wano, Wino, SAMPLE PRIORITY [dnour1ME □EMEllGlcNCY -13Jcl-l/\lN OF CUSTODY wsno, l<inslon ro, ~I. Trusl, Cenlral 011., Other: _________ _ Sl1ipped by: Bus,~. I-land Del., Other.,·~----------- 0 '"" """'"~Q'J'.i',I Dale neceived l _ .\'.i1.__ Time ,,d;:-'--"'---'="'---- nec·d by:_ f"'rom: l3u. nun OIiier: __________________ _ Dala E11lry l3y: ______ Ck: ______ _ , I land Del., Dale neprnled: ______________ _ "-l.j/,71--·•-, . Pwpose: Collector(s):. ¥,:6,,( <-oo Date ~2(__]_'---. Time /J. '-tJ~ __ Baselino, Complainl, Compliance, LUST, Peslicido Study, Federal T,usl. Ollie,: ,~uclo 01101 FIELD ANALYSES Owner _fir,~ c, r_s;._,;_dds..~-~---~-----~---------------- pl-l,00 S-::-y: J-Spec. Co11d.9, fl O al~&' C Location or sile tig!:, / 77 (_,: ~ct'.~ U,, ~ , .Jfcic, ., IG Ternp.10 • °C Odor_______ Description of sampling point 5,e.-,,,t c {,;__;j_ "-r.:, 4c, ~ -, ✓ ~ Appeara11ce cC<4--/,~J,-w;· Sampling Melhod -------~r -:::,.,\_ .. -~--------Sample l11lerval ________ _ f'ield Analysis By: '.U<:' {, ie,, llemarks le:( ~'-n ~) -irtJ.----~-''_'"'_'_·_'''.'1 ':c'·="'=':::' ===c:--:=-------------------LABORATORY ANALYSES lpomp"'"""-'"""''·'"1 BOD, 310 mg/I Diss. Solids 70300 mq/1 J\g • Silver 4G566 ug1 Organocl1lori11e Pesticides --COD High 340 mgll Flouride 951 mntL /\I -Aluminum -16557 uu~ Orgt111opl1□srl1orus l)eslicides ----------------COD Low 335 mg/I Hmdness: Total 900 l!lQ!L As -Arsenic 46551 uq/1 Nilrogen Peslicitles -----Colilorm: MF Fecal 31616 1100ml Hardness {non-carb} 902 mgll Ua -Barium 46558 uqtl Colifor rn: MF Tolal 31504 1100ml Phenols 32730 u_g1L Ca -Calcium 46552 111(]1! Acid Her bide.Jes --lOC Gao 111911 S2gecilic Cond. 95 uMl10s/crn~ Cd -Cadmium 46559 ugtl --Tu1bidi1y 76 NTU Sulfale 94S mg/I Cr -Chromium 46560 uqll Semivolatile Organics --Residue., Suspended 530 mg/I Sulfide 745 11191_ _g_u -C~r?rer 46562 ug~ ---- r-e -hon 4G5GJ ugll --y x -------I-lg -Mercu,}:'. 71900 ug/1 Volnlile Organics (VOA bollle) pll 403 unils K • Potassium 46555 mgtl ----. /llkalini1y lo pH 4 .5 410 mg/I -~9....:__~!:_!Unesium 46554 1119{1 TPH -Gasoline nange ------/llkalinity lo pl! 0.3 415 1119/~ -~•~_i!(~U<HlCSO 4G5G5 ug{!_ TPI I -01 EX Gasoline flange ---------Cmlmnato '145 mgll NII, as N G10 mq/1 Na -Sodium 46556 mg{I Bicarbonale 440 mg/I .TKt:Las..N_i;2s 11\J/I. Ni -Nickel ugQ ------Ca,bon dioxide 405 mg1! X NO" + N0;1_as_N GJO f!]gl! J~b -Lg~f!__1fi5G-1 un(! ~I ------Chloride 940 1119/I P: Tolal as P 665 rng!I So -Selenium ug~! --Chromium: Hex 1032 ugll Zn -Zinc 46567 u91 ----Color: True oo Pl-Co ----Cyanide 720 mg/I Lab Comments: ------------------~--------------------------------------- GW-S4 nEv. G.'93 For Dissolved Analysis -subn1il filtered sample .ind wrile "DIS" in block. - -- REPORlED BY CHECKED BY REVIEWED BY SAMPLE TYPE: 75-35-4 75-09-2 156-60-5 75-34-3 590-20-7 156-59-4 67-66-3 74-97-5 71-55-6 563-58-6 56-23-5 107-06-2 79-01-6 78-87-5 75-27-4 74-95-3 10061-01-5 10061-02-6 79-00-5 127-18-4 142-28-9 124-48-1 106-93-4 108-90-7 630-20-6 75-25-2 79-34-5 TOL- T- E- U- N- 0- M- COMMENrs· - ---- WAIER 1, 1-Dichloroethene 0.75 Methylene Chloride 10 lrans-1,2-Did11oroe1hene 0.75 I. 1-DichloroeHmne 0.25 2,2-Dicliloropmpane 0.25 cis-1,2-0ichloroethene 0.25 Chloroform 0.25 Bromochloromelhane 0.75 1, 1. 1-Trichloroelhane 0.25 1. 1-0ichlorop,opene 0.25 Carbon Tetracllloride 0. 75 1.2-Dicllloroelhane 0 25 lricl1loroethene 0.25 1. 2-0ichloropropane 0.25 Bromodichloromethane 0.25 Dibrornomelhane cis-1,3-Dichloropropene 0.25 trans-1,3-0ichloropropene 0.25 1, 1,2-Trichloroethane 0.25 T etrachloroethene 0.25 1, 3-0ichloropropane 0.25 Dibromochloromethane 0.75 1.2-Dibromoethane 1 Chlorobenzene 0.25 1, 1.1.2-T'etrachloroethane 0.25 Bromolorm 0.5 1, 1,2,2-1 etrachloroethane 0.75 Targel Quanlitation limi1-Subject to change due lo instrument sensitivity Tentatively Identified. not confirmed Estimated Value Samples analyzed for lhis compound but nol detected Sample not analyzed for this compound Detected below quanlilation limit GC/MS Analysis performed - - - EIIUR/DWQ LAO ORA lORY VOLATILE AtlALYTICAL REPOFH AUALYSIS RESULTS u 96-18-4 u 108-86-1 u 95-49-8 0,59 106-43-4 u 541-73-1 1.3 E 106-46-7 II 95-50-1 - - - 1.2,3-T 1ich1oroprnpane Bromobenzene 2-Chlorolo!uene 4-Clllorotohicne 1,3-Dichloiobenzene 1,4-0ichlorobenzene 1.2-Diclilorobenzene u 96-12-8 1, 2-Dibromo-3-Ch!oropropane II 120-82-1 1,2,'1-l richlorohenlene u 87-68-3 I te)(achlorobutadiene II 87-61-6 1.2,3· lrid1!orollenze11e II 1634-04-'1 Me111yl-1erl·ll•1\yl eU1er u 71-43-2 Benzene II 108-88-3 TohlC!ne II 100-'11-'1 Ett1yl benzene u 108-38-3 m,p-Xylenes u 95-4 7-6 a-Xylene u 100-42-5 Styrene u 98-82-8 lsopropylbenzene u 103-65-1 n-Propylbenzene u 108-67-8 1.3.5-Trirnethy!benzene u 9B-06-6 tert-Buty1benzene u 95-63-6 1.2.4-l rimethylbenzene u 135-98-8 sec-Bulylbenzene u 99-B7-6 p-isopropyUoluene u 104-51-8 n-Butylbenzene u 91-20-3 Naphthalene Gasoline Range Estimaled Total Petroleum Hydrocarbon Ollie, pu19eables detected (up to 1 O highest peaks) NO VOLA l lLE ORGANIC COMPOUNDS DETECl ED BY GC/PID. ---LAB MO. 7G07B1 SU!'EHVISOH rJ?.it.. · __ DAIE ~2!1/il ENIEREDA';~--- DAIE_.!cj_.d:_:~, 0.25 u u 0 25 u 0 25 u 0 25 u 0 25 u 0 25 u ll 0.25 u 0 25 u 0 75 II 5 II u II I u 2 u u u u u u u u u u u u mg/l mg/l 0 25 N Detecled ug/L :--,- I I I I I I I I I I REFERENCE 19 I I I I I I I I I . I. I I I I I I I I I I I I I I ; I I I I' Ref. 19 $tate of North Carolina Department of Environment, Health, and Natural Resources 512 North Salisbury Street • Raleigh, North Carolina 27604 Division of Solid Waste Management James B. Hunt, Jr., Governor Chris Davidson P.O. Box 5602 Statesville, NC 28677 Dear Mr. Davidson: Telephone 919-733-2178 February 22, 1993 . ' Jonathan B. Howes, Secretary \:. ·>:j· \:l (', /'.'!,. ~--c..i~-· ·,· Please find enclosed the analytical results of the water sampled from your well on September 1, 1992. Reportedly, this well is no longer used for drinking water. The sample collected from this well contained iron (4.43 mg/1) and manganese (0.83) at concentrations which exceed the North Carolina water quality standards for ground water (Title 15: Subchapter 2L .0200). If you have any questions, please call me at (919) 733-2178. Sincerely, ~~-)~ Laurie Martin, Hydrogeologist Ground Water Unit Hazardous Waste Section cc: central files Jesse Wells P.O. Box 27657, Raleigh, North Carolina 27611-7687 Tdephone 919-733-4984 Fax # 9!9-733-0513 An Equal Opportunity Affirmative Action Employer n D I I I I I I I I I I I I I I I I SAMPLE ANALYSIS REQUEST r,.r. D·partmcnl of Environment, I lcaHh, & Natural Rcwurccs Solid Wutc Management Division State Ubora1ory of Public Health P.O. Boi 28047, 306 N. Wilming,on Strccl '\ Ralciih, North Carolin• 27611 . . {_ ) V ,J.1 V· ) I_) ,! ·,_ Sile Number r" .)/0:v..,1.:, 11 ) , \(' efz,:-(, tC Field Sample Number _____ _,_-'----------- / ' Name of Sile ---------------- /( Agency: (_ Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Site Location {-_ U {t' In. ------'--'--'---'------------- Date Collected 1/ /; /9? Time ( ( 5 (_, ---'-f-,-'--'-------'------ Sample Type lnor;:anlc Compounds Results(mg/1) Environmental Concentrate Commrnts Arsenic --Barium l/ Ground water (1) /\ I I ,,. --Cadmium _ Solid (5) ,. ' .. \ I' I-/ -'-1\ :\ :.:u..::,. ..... --Chromium --Lead Surface water (2) _ Liquid (6) ----Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --__ Other (4) Other (8) ---- --Organic Chemistry Inorganic Chemistry -- Parameter Resull5(mg/l) Parameter Results(mg/1) (mg/kg) Organlc Compound• Re,ults(mg/1) .i.::::_ P&T:GC/MS Arsenic benzene _i.___:'Acid:B/N Ext. ----carbon tetrachloride Barium ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ---- --__ Copper o-cresol --Fluoride m-cresol ----= p-cresol --Iron --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury 1,2-dichloroethane --Nitrate --1,1-dichloroethylene --Selenium 2,4-dinitrotoluene --Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-· Zinc hexachlorobutadiene --ftarumt'tt'r Results (PCl/1) _pH hexachloroethane __ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ----= pentachlorophenol TOC ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parumeter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichloropheaol ----__ vinyl chloride endrin -- SEP 2 E92 eS> lindane Datt Received --Reported by __ methoxychlor __ toxaphene Date ExlractcJCi-'-/ ~,, ;,_A QI' I<; Date Reported 2,4-D )) ' , ,., ·-' --"'~r-"T"ntr-•1 ___ '\ I I I P\J!lGEAB LE C0'1POJNOS CD1PO.JIID I ch lorD'Tl'!thane "'•O'TO'nethane ichlorodifluoronethane I vinyl chloride chloroethane ethvlene chloride rlchlorofluorc:methane n ethene 1 1-dichloro ~th.me. 1 1-dichloro- 2-trans-dichloroethene 0 chloroform U ethane 1.2--dichlor6- thane l.1.1-trichloro-II .art>ontetrachloride II brOTOdichlororethane rooan-e 1-2-dichloro- . 3-trans--d i ch 1 oroon::oen-e 11 trichloroethvlene II ·arodibrororethane I ethane l l 2 trichloro-- 1 3--<:is--<Jichloroorcoene --chloro,ethvl vinvl ether I ..:rorof or.n ethane 1 l 2.2-tetrachloro- thene tetra ch l oro- oluene I chlarcoenzene ·thvlb,enzene I acetone 7-butanone .artxmdisulfide STATE LABORI\IORY Of rvouc HEAL DIVIS ION Of HE!-LIH SERVICES, N.C. OEPAAIMEHT C .HUIWl RESCURCES P.O. BOX 28047 -306 N. l<ILMIHGTON, Sl., RAL IGH, H.C. 21611 FIELD I I TYPE UNITS I ~/ t; ...... --. h I . , ./ I iOooh I ,; -~h O'lc:ANIC CHEMICAL ANALYSIS ' / CT '.)lOl1 11_,;J I I l-J . .j"., ( I \ <. \ ) ( I ( ) ( ) ( ) (Uo/ l ,AJo/ko · uo/ 1} uo/ka tGo/1 >t.lo/ko vo/1 va/k'.o uo/1 uo/ko uo/l uo/ko I' I I I ..J.-,.-.,r,. _ I I I I ---J J _i.,...r, ,. ,.. J._, .• ,.,,. •· ; I ,t..-,, ,·r I I I I I I I I I I I I I I I I I I I · , 1 I ,/ I , / I I I I I I I I I }" ~~ h u ) ' I-~-I I :i, I I I ,.../\exanone \ IO OQD I I _L,,-e:--"'-'t"hv:..l:...-..=2.=--oe=n'-'t"'a"'no>'.!.'.ne:..... ___ -1--1·1_' --+-----+-------t----'!---+-----+--------;-1-----tvrene \ I I •invl acetate ,vlenes fh,i-0 /J ,1 . I •.. ------l----1---+----l----1---+-----+:-- 'fMDL1' I Estimated value. Actual value is kno.m to be less than value given. 1 -.:... Actual value· is t'no,.,n to be greater than value given. -l'\aterial \Jas analyz~ for but not detected. The nUTber is the M.lnim..rn Detection Limit. = MDL \ -Not analyzed. 11/ -Tentative identirication. · , 21 -On HROC _List cf Priority Pollutants. J ·.c. Division of !t~alth s~rvices l I I STATE LABORATORY Of PUBLIC HEALTH D!V!S100 Of HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOJRCES I P.O. BOX 2'8047 -306 N. _W!LHINGlOO, Sl., RALEIGH, N.C. 27611 -----------,-----,-,=;-,,-,~OO'"GAN77I~C,.;()j7"-E!,'-Hl~CA7':L-:;'Afl"i"A'-'L;-YS"'I',;S':7-..,-;--,,----,,----,---- BI\SE/HEUl RAL NID ACID LAB HO -/_?_,;,,) I.· Cf.)_.).'j] 7 "1..-!,:)-J.J V EXTRACTABLES FIELD # / / J...). ,·, // ,_-,_ -, I J / ,J . .J '- CDMPOJND TYPE ( / ) l I ) f I ) UNITS uo/] ,,iQ/ko uo/1 iJQ/l<:o uo/1 \,oAo uo/1 uo/ko ( l ( ) ( ) uo/ 1 uo/ko uo/ 1 uo/ko -nltrosodirrethvlamlne is (2-eh loroethvl let her I I -eh l ol'YY\heno l I I lenol I I ,3-dichlorobenzene I I i-dichlorobenzene ! I : 2--<Ji ch 1 orobenzene I I . s (2-eh 1 oro i sooroovl lether exachloroethane -n i t roso-d i -n-or(Y')v 1 amine trobenzene soohorone -nitrooheool 4--<J irrethvl pheno 1 is (2-eh loroethoxvlrrethane 4--<Jichloroohenol 2. 4-tri ch lorobenzene whtha Jene exachlorobutadiene ,loro-m-eresol :xachlorocvclooentadiene 4.6-trichloroohenol -ehloronaohthalene :enaohthvlene irrethvl ohthalate 6-dinitrotoluene :enaohthene 4--<Jinitronhenol SO//<,So 4--<Jinitrotoluene -nit NY"lheno l luorene -chloroohenvlohenvlether I iethvl ohthalate J, ,6-dinitro-o-cresol iohenvlamlne /0/330 zobenzene ' -bronoohenv 1 ohenvl ether ?xach l orobenzene ntach lorooheno 1 1enanthrene 1thracen-e ibutvl ohthalate I, luoranthene \ V nYDL I. Estimated value. l{,_o/sou .... -Actual value is known to be less than value given. Actual value is known to be greater than value given. -Material was analyze<l for but not detecte<l. !he nurber P, -Not analyzed. is the Minilll.lTI Detection Limit. rn1JL --- -~ -lentative identification. 1 -On NROC List of Priority Pollutants. - I I I n I I I I I I I I I I I I BASE/NEUTRAL ANO ACID EXTRACTABLES CD'IP(JJHD n.vrene benzidine butvl benzvl nhthalale ben z r a 1 an thracene chr'-'Sene 3 3-dichlorcbcnzidirte bis(2-,,thvlhexvl'nhthalale di-n-octvl nhthalate benzo 'bl fluoran thene benzo(k)fluoranth<ane benzo(a~rene i ndeno{ 1 2 3-ed) '"'"rene dibenzo(a h)anthracene benzoln h i'=rvlene aniline benzo 1C aCl d benzvl al coho 1 4-chloroaniline dibenzofuran 2-nethvlnaahthaTene 2-nethvlnh<,ool 4-methvl ph<,oo 1 2-nitroanlline 3-nitroaniline 4-fl i troan i 1 i ne 2 4 5-trichlorooh<aool J -Estimated value. STATE LABOOATOOY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, H.C. DEPAR1HEN1 OF HUIV\N RESOJ~CES P.O. BOX 28047 -306 H. W!LHIHGTON, ST., RALEIGH, N.C. 27&11 OOGANIC ~EH!CAL ANALYSIS LAB HO (l.~,2';1 /_ '-f_:J·~''-t-' } v,.Y-J../? r· FIELD • -1 I.,_ J.---' I 1.1. J. I r'✓:2 .:,__i. TYPE I/ l I i l I ( l ( l UNITS · ;.n/ 1 --._✓k-0 .. n/ t) •-lko .. n/ 0-nlka un/l .. n/ko /o/o:;~ --.,,,_ ____ ;, l.....-I,<_,. '" /,1.,;o I /0/"30 i • I, so/1t-.r;,, /o/33n /0/3:.o sol11,,,o \ ·, ' \7 \ ' <o/1t-.ro (,<._... !A--ilL- I ~ r /0 /=r. ,r, :;0 7,1 .. c0 ,,, I , •7 to be less than value glven. to be greater than value given. for but not detected. lhe nlft'bc-r is the t1inirn..JT1 Detection Limit. ~ -Actual value ls known l -Actual value ls known 0 -Katerial was analyzed NA .. Not ,malyzed. 1.' -tentative ident\flcation. £1 -On HROC List or Priority Pollutants. N.C. D.i.v.u.i.011 "' Kr.a.Uh SVtv.i.cv., ( l ( ) uo/ l 00n/ko uQ/ 1 .. n/b I I I I I I I I I I I I I I I I I I I N.C. Department of Environment, I lc:il~h, &. Na1ural Retourre~ Solid Wute Man.agemcnl Division !,,.MPLE ANALYSIS REQUEST State Laboratory or Public Health P.O. Box 28047, 306 N, WiJminiton St~c:1 R.alciJh, North Carolina 27611 Site Number ----------------Field Sample Number _____ {J;.:....:;u::.....,7::......2"--------- Name of Site .f/6,., Ml / ,',4 r7,.',.-{ ,f, 5',c'/"/7cM,,-1(2 ,;-a,,J /ZL.Ylte 'Location __ ---'h'-=l./<-Cb::s:,,.::L:..c.4:..,_ _________ _ / * /2 Collected By (rL~)/h-"f:77J,~ ID# I Dale CoUecled '7// pz_ Time !.i..se , ; Agency: ~Hazardous Waste Solid Waste __ Superfund TCLP Compounds -- Sample Type Inorganic Compound., Results(mg/1) Environmental Concentrate Comments Arsenic --Barium _~ound water (1) --Cadmium _ Solid (5) --Chromium --__ Surface water (2) _ Liquid i6) Lead ----Mercury Soil (3) _ Sludge (7) Selenium --Silver --Other ( 4) _ Other (8) Organic Chemistry Inorganic Chemistry Parnmeter Result.,(mg/1) Parameter ~sults(mg/1) (lllB,'I"' Organic Compounds Results(mg/1) --P&T.GC/MS / Arsenic ( o. Q'f benzene ----Acid:B/N Ext. V Barium Q_e,7 carbon tetrachloride MTBE 1/Cadmium <o. Ql./ --chlordane --------1L:Chloride -,,:_5 chlorobenzene VChromium <o. OY --chloroform -- (/'Copper ----0-0lc o-cresol --V Fluoride ----Q - \ \ m-cresol --:;r Iron '--\ . .,;::i = p-cresol ----...J.L Lead <' o_. QY. cresol ----...JL Manganese o_ 'o 3 --1,4-dichlorobenu:ne --...J..L Mercury o.oa) 1,2-dichloroelhane --_u'.'.._ Nitrate ..::.. 1-QO = 1,1-dichloroelhylene £Selenium < o. OIJ_ 2,4-dinilrololuene ....1L... Silver L...o.oe;:. heplachlor Radiochemistry ..JL. Sulfates (..._ bexachlorobenzene --..LZinc -L.o.o5:'.> hexachlorobutadiene --Par.1meter Results (PCl/1) t/ pH c.;2_"?-~i s hexachloroethane __ Gross Alpha .JL Conductivity methyl ethyl ketone Gross Bela t/ TDS 2?: d-, --nitrobenzene --[/TOC £:vvti~...._~,, -f-'-t.l.l~ __ penlachlorophenol __ pyridine --Microbiology --__ telrachloroclhylene --__ Lrichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-Lrichlorophenol ------__ 2,4,6-trichlorophenol --. __ vinyl chloride endrin --lindane Dale Received Reported by __ melhoxychlor __ Loxaphene Dale Exlraclcd Dale Reported 2,4-D --2,4,5-TP (Silvex) Dal c Analy,cd Lab Number -- 1 .. I .---, I __ , D D I I I I I I I I I I I State of North Carolina Deportment of Environment. He.alth and Natural Resources M_ooresville Regional Office James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary DIVISION OF ENVIRONMENTAL MANAGEMENT December 14, 1995 Davidson Roofing Company Buffalo Shoals Road Statesville, North Carolina 28677 Attention: Chris Davidson Dear Mr. Davidson: RE: Well Water Sample Results Davidson Wells Iredell County, N.C. On October 10, 1995, staff from the Mooresville Regional Office of the North Carolina Division of Envirorunental Management sampled the well at Davidson Roofing Company and the well at your residence. The samples from the well at the roofing company were collected at 173 Lauren Drive. Samples from both wells were analyzed for volatile organic compounds, mercury and nitrate/nitrite. Volatile organic compounds include a wide range of manmade compounds including, but not limited to, gasoline components and chlorinated solvents used as degreasers. Laboratory results from these samples indicate at the time of sampling that neither mercury nor volatile organic co~pounds, were present in the roofing company well. In addition, the level of nitrate/nitrite was 1.4 parts per million (ppm), which is less than the EPA Dri~~ing Water Standard of 10 ppm. Laboratory results from the samples collected from the well located at your residence indicate at the time of sampling that mercury was not present in the water supply. However, tetrachloroethene, a volatile organic compo .. 1d, was detected at a level less than the EPA Drinking Water Standard of 5 parts per billion (ppb). Again, the nitrate/nitrite level of 1.4 ppm present in your residential well does not exceed the EPA Drinking Water Standard of 10 ppm. Should you have any questions, please call me at (704) 663- 1699, ext. 243. Enclosure: Lab Results sincerely, k0,ll11 tn,,lLll Karen Connell Hydrogeologist cc: Iredell County Health Department 919 North r-✓1oin Street. iv'looresville. f'1orth Carolina 26115 Mn t:quol Oopor."-Jn:;y .A.~1,;notive ,:.c:ion f:;:1plover I elephone 704-663-i 699 F.0.x 70<l-663-60<lC North Caroll no GROUNDWATER FIELD/LAB FORM Oopartment of Environment, Health, end Natural Aosource'.'I OF ENVIRONMENTAL MANAGEMENT-GROUNDWATER SECTION County \-' Q -90d el( Ouad No Lln1h Serial No_______ SAMPLE PRIORITY niv':1-' Lat. -S~6,_"_' _4_,__3'"'-' D"-'-J _' 1_ Long_ go c .5 '/ 1 -5 </-11 · -fJ.?lROUTINE □EMERGENCY,-,,,;,_ -------l'.'.:.l Other: w ~ , M CHAIN OF CUSTODY -;:. l 1, ~ Report To: ARO, FR0,@9, RRO, WaRO, WiRO, l6J -1' -~ Data Entry By: / ~ Ck:,-.~~---- WSRO, Kinston FO, Fed. Trust, Central Off., Other:_________ , , .,,;, ,,,,;;Qa.r Reported: _~/_:V_F-~1/,;~z'_o _______ _ Shipped by: Bus,~_ef', Hand Del., Other·_____________ N1i\\ci._ 1'1, t~i-_ ,,,,;,;0 .,.,Hi;; "' _ ~-'_'tf', Purp0se: ~rn.,11"" 1-olL' ~kc# .Jy:;; :i, Collector(s): 1<,C1:Y1nE ll Date /0 /ID /q 5 Time (J · :;5 P"l Baseline, Complaint, Compliance( LUST, Pesticide Study, Federal Trust, Other: Poll cd; 6n 1101,, i c•; _, . . /J . c11d1 Ont) FIELD ANALYSES Owner 8i;u.,J t.h,],cl:::n'YJ 1&01QJ1?1-(,G pH,oo _____ Spec. Cond .• , ----at~S° C Location or site ¢!f 1ro9 -,,5/cclo=c~•iLl~Le,,.~-,---,--c------c-------------------- Temp.,o --~--0c Odor ,,__,_J.P=N~-----Description of sampling point hose 6ihb oa /:nck o+ /;Q((S"- Appearance Wcv1 Sampling Method P_t<~n_P ____ ~-~~~~~-------Sample Interval /,lA.l'1o,cn l/,-"'7 Remarks ,led aP•,,~ · tP~mp_s.,i., .• ,"i Field Analysis By: ,_rv~L~D'--n-"n'-'-'-Q_,.1,_,_,_________ c, i::· LABORATORY ANALYSES BOO 310 mo/I Diss. Solids 70300 mn< Aq • Silver 46566 uni! Organochlorine Pesticides· COO High 340 mg/l Flourido 951 mnA Al -Aluminum 46557 ugil_ Organophosphorus Pesticides COO Low 335 mall Hardness· Total 900 m"'I As -Arsenic 46551 uall Nitroqon Pesticides Coli/arm: MF Fecal 31616 /100ml Hardness (non-carb) 902 mqll Ba -Barium 46558 ug/1 Coliform: MF Total 31504 /100ml Phenols 3i73o u~I Ca -Calcium 46552 mall Acid Herbicides TOG 680 ma1 I ,_ Specific Cond. 95 uMhos/cm2 Cd -Cadmium 46559 uall Turbidity 76 NTU Sul/ale 945 mnl\ Cr -Chromium 46560 uo/1 Semivolatile Organics Residue., Suspended 530 mg/I Sulfide 745 mall Cu -Copper 46562 uall Fe -lron 46563 uq/I X Hq -Mercury 71900 L()_-:) uq/I / Volatile Organics (VOA bollle) pH 403 unit~ K -Potassium 46555 mg!I Alkalinity lo pH 4.5 4\0 mg/I Mg -Mc1gnesium 46SS4 mg/I TPH -Gasoline Range Alkalinity 10 pH 8.3 4\5 mg/I Mn -Manoanese 46565 uc/11 TPH -BTEX Gasoline Range CarOOnate 445 mg/I NH as N 610 tJ. o-sc ma..l Na -Sodium 46556 mall Bicarbonate 440 mail ITKN os N sos mQI.L Ni -Nickel unA Carbon dioxide 405 moll :>< NO + NO as N 630 /,-;/ mnA Pb -Lead 46564 uo/1 ( / Chloride 940 mg/I P: Total as P 665 ma/I Se -Selenium uo/1 I/ Chromium: Hex 1032 uall Zn -Zinc 46567 uo/1 - -Color.: True ea Pt-Co Cyanide 720 mg/I _ Lab Cor;iments: ------------------------------------------------------- l!!!!!I l:l:llssolliiiliif1a1y,aon"•-u ><>all'"" lilli---111111 ------' -.. - EHNR/DEM LABORATORY LAB NO. 501749 ~ VOLATILE ANALYTICAL REPOR ." REPORTED BY SUPERVISOR CHECKED BY DATE l/tI REVIEWED BY ENTERED BY / 3/ _!;✓-~5' CHECKED BY ~ SAMPLE TYPE: WATER ANALYSIS RESULTS 75-35-4 1, 1-Dichloroethene 0.75 u 96-18-4 1, 2, 3· T richloropropano 0.25 u 75-09-2 Methylene Chloride 10 u 108-86-1 Brornobenzene 1 u 1 56-60-5 trans-1, 2-Dichloroethene 0.75 u 95-49-8 2-Chloroto!uene 0.25 u 75-34-3 1, 1-Dichloroethane 0.25 u 1 06-43-4 4-Chlorotoluene 0.25 u 590-20-7 2, 2-Dich1oropropane 0.25 u 541-73-1 1,3-Dichlorobenzene 0.25 u 156-59-4 cis-1. 2-Dichloroethene 0.25 u 106-46-7 1,4-Dichlorobenzene 0.25 u 67-66-3 Chloroform 0.25 u 95-50-1 1, 2-Dichlorobenzene 0.25 u 74-97-5 Bromochlororne thane 0.75 u 96-12-8 1, 2-Dibrorno-3-Chloropropane u 71-55-6 1, 1, 1-Trichloroethane 0.25 u 120-82-1 1,2,4-Trichlorobenzene 0.25 u 563-58-6 1, 1-Dichloropropene 0.25 u 87-68-3 H oxachlorobut adio ne 0.25 u 56-23-5 · Carbon Tetrachloride 0.75 u 87-61-6 1 ,2, 3-T richlorobenzene 0. 75 u 107-06-2 1,2-Dichloroethane 0.25 u 1634-04-4 Methyl-tert-butyl ether 5 u 79-01-6 Trichloroethane 0.25 u 71-43-2 Bonzene u 78-87-5 1, 2-Dichloropropane 0.25 u 1 08-88-3 Toluene u 75-27-4 Bromodichloromethane 0.25 u 100-41-4 Ethyl benzene u 74-95-3 Dibromomethane 1 u 108-38-3 m,p-Xylenes 2 u 10061-01-5 cis-1, 3-Dichloropropene 0.25 u 95-47-6 a-Xylene 1 u 10061-02-6 trans-1,3-Dichloropropene 0.25 u 100-42-5 Styrene u 79-00-5 1, 1,2-Trichloroethane 0.25 u 98-82-8 lsopropylbenzene u 127-18-4 T etrachloroethene 0.25 D 103-65-1 n-Propylbenzene u 142-28-9 1, 3-Dichloropropane 0.25 u 108-67-8 1 ,3, 5-Trimethylbenzene u i 24-48-1 Dibromochloromethane 0.75 u 98-06-6 ter(-8uty1benzene u 106-93-4 1, 2-Dibromoethane 1 u 95-63-6 1,2,4·Tdmethylbenzene u 108-90-7 Chlorobenzene 0.25 u 1 35-98-8 sec-Butylbenzene u 630-20-6 1, 1, 1,2-Tetrachloro·ethane 0.25 u 99-87-6 p-isopropyl toluene u 75-25-2 Bromoforrn 0.5 u I 04-51-8 n-Butylbenzeno u 79-34-5 1, 1,2,2-Tetrachloroethane 0. 75 u 91-20-3 Naphtha!e~e u TOL-Target Ouantitation Limit-Subject to Other purgeables detected Detected change due to instrument sensitivity (up to 10 highest peaks) ug/L T-Tentatively Identified, not confirmed E-Estimated Value NO VOLATILE ORGANIC COMPOUNDS DETECTED BY U-Samples analyzed for this compound but not detected GC/PID. N-Sample not analyzed for this compound 0-Detected below quantitation limit M· GC/MS Analysis performed --""MM,"---- ' : : 1!!!11:11 == i=;;i liiiiil iiiii -- - -------- - -- CHAIN OF tment of Environment, Health, find Nature! Resource:, GROUNDWATER FIELD/LAB FORM C ~~J-oo~· . , o r t h C a r o I I n a I I NVIRONMENTAL MANAGEMENT-GROUNDWATER SECTION Lab Number 5C--. ~\J County \cY!l!ld,r../'..L Ouad No L l,, '1,.,-, Lat. 35c L/)' 5q 11 Serial No. _______ _ Long. 80° 5? 1 c,1./ 11 lvlROUTINE □EMERGcNCY Rec'd by: \LP ~rom: Bu~ Hand Del., SAMPLE PRIORITY O Date Rece~Y.e9 ...,\D.\Jl\fiTimeJQ:9:::) l'.:o.J Other: ---~~-------------~:,_ acHAIN OF cusTODY l-----:,1 ~ Report To: ARO, FRO.~,HRO, WaRO, WiRO, l::'.\.J Data Entry By: ,i__ Ck:~ WSRO, Kinston FO, Fed. Trust, Central Off., Other:_________ Date Reported! J 15 /9 '::i.- Shipped by: Bus~_ rieJ, Hand Del., Other·____________ 9jH'.l,,u. ·Jr ,jy;:i::,, ~u;~[r" I . • Purpc,se: Collector(s): KC on, tx. Date -1Qj /Ojq5 Time I;) ,[Opm Basoline, Complaint, Comprance, LUST, Peslicide Study, Fedor el Trust, Other: E,llw;1,, llt·1ccftr; ·"· . i i\ \CIIC11 Or>O) {j FIELD ANALYSES owner Dcw,ct~o., R,_,,-, cl.{_ 1-x=,,,_ ucw, ~ R.c.csfi,.,, c. pH 400 (g. 0 Spec. Cond.94 i/0 u'1 l,vs at;\:° c Location or site i '13 J a.cVU/n L1u.~ Temp.10 -~Q'-'3=... __ 0 c Odor Vl,/'f4' Description of sampling point l'LQ;t b:ihr1 cm Q(d,~ C lux<oz... Appearance Sampling Method Pt.unp Sample lnterval__:_c_,,.,c:k.-=-:.· ____ _ K n 1' (],... I _1 (Pump, W,1181, lillC) .~ I D . Field Analysis By:((Ypf1.Q,:,< Remarks 0'.LiY'p ev. QiCQ;) p.LL:n14-rn><./b=.,£..'fl==°=~~--"'-~mC.'cC1\'-Jnul _____________ _ S S 1 \ I/ aJ: Iv; f: C,. \ 7ifump"9 om,.•• ""'P '"1 LABOB6IOBY 6NALY E ,LL , ·c1 ,nci l M /1 llAl..l. l- BOD 3)0 mall Diss. Solids 70300 mall Aq • Silver 46566 U"" Orqanochlorine Pesticides COD High 340 mg/I Flouride 951 mo> Al -Aluminum 46557 urul Organophosphorus Pesticides COD Low 335 mall Hardness: Total 900 mgll As -Arsenic 46551 uall Nitro□en Pesticides Coliform: MF Fecal 31616 1100ml Hardness fnon-carbl 902 mall Ba -Barium 46558 UQ/1 Coli[orm: MF Total 31504 1100ml Phenols 32730 uall Ca • Calcium 46552 mail Acid Horbicides TOG 680 mail -Sgecific Cond. 95 uMhos/cm1. Cd -Cadmium 46559 uca Turbidity 76 NTU Sulfate 945 mg/I Cr -Chromium 46560 unil Somivolalile Organics Residue., Suspended 530 mg/I Sulfide 745 m0/1 Cu -Conner 46562 """ Fe -Iron 46563 uca ,>< Hq • Mercu,y 71900 < {). 7 uni '>< Volatile Organics (VOA bollle) pH 403 unit~ K -Potassium 46555 ma,I Alkalinity lo pH 4.5 410 mgll Mg -Magnesium 46554 mg,'I TPH -G.iso!ine nango Alkalinily lo pH 8.3 415 mg/I Mn -Manqanese 46565 un.l TPH -BT~X Gasoline Range Carbonale 445 mg/I NH asN 610 L'O, O I mail Na -Sodium 46556 mrul Bicarbonate 440 m"" J'.KtlasJ'LJiZ' moLJ_ Ni -Nickel ug!I --/, I /, ,-., .,,-,,··· -~ Carbon dioxide 405 mon X NO + NO as N 630 y mail Pb. Lead 46564 uca Chloride 940 mgll P: Tolal as P 665 mall Se • Selenium """ bdvrnn";\1 ~,.,·;-, I Ir.-'-I.TH Chromium: Hex 1032 ug/1 Zn -Zinc 46567 urul & NATU:? ... \L 1<~'.~;CJt::,,·:1~:l ,- Color: True eo Pt-Co .. ::-: a h ·,., Cyanide 720 mgll NOV ---- - --11111111 ... - REPORTED BY CHECKED BY REVIEWED BY SAMPLE TYPE: 75-35-4 75-09-2 1 56-60-5 75-34-3 590-20-7 156-59-4 67-66-3 74-97-5 71-55-6 563-58-6 56-23-5 107-06-2 79-01-6 78-87-5 75-27-4 74-95-3 10061-01-5 10061-02-6 79-00-5 127-18-4 142-28-9 124-48-1 1 06-93-4 108-90-7 630-20-6 75-25-2 79-34-5 TOL- ~ WATER 1, 1-Dichloroethene Methylene Chloride trans-1, 2-Dichloroethene 1, 1-0ichloroethane 2, 2-Dichloropropane cis-1,2-Dichloroethene Chloroform Bromochloromett1ane 1, 1, 1-Trichloroethane 1, 1-Dichloropropene Carbon Tetrachloride 1, 2-Dichloroethane Trichloroethene 1, 2-0ichloropropane Bromodichloromethane Dibromomethane cis-1, 3-Dichloropropene trans-1,3-Dichloropropene 1, 1,2-Trichloroethane T etrachloroethene 1,3-0ich!oropropane Dibrornochloromethane 1,~-0ibromoethane Chlorobenzene 1, 1, 1,2-Tetrachloroethane Bromoform 1, 1 ,2,2-T etrachtoroethane Target Ouantitation Limit-Subject to change due to instrument sensitivity T-Tentatively Identified, not confirmed Estimated Value 0.75 10 0.75 0.25 0.25 0.25 0.25 0.75 0.25 0.25 0.75 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.75 0.25 0.25 0.5 0.75 E- U- N- Samples analyzed for this compound but not detected Sample not analyzed for this compound D-Detected below quantitation limit M-GC/MS Analysis performed WWW --- EHNRIDEM LA BORA TORY VOLATILE ANALYTICAL REPORT - ANALYSIS RES UL TS u u u u u u u u u u u u u u u u u u u u u u u u u u u - 96-18-4 108-86-1 95-49-8 106-43-4 541-73-1 1 06-46-7 95-50-1 96-1 2-8 120-82-1 87-68-3 87-61-6 1634-04-4 71-43-2 108-88-3 100-4 1-4 1 08-3B-3 95-47-6 1 00-42-5 98-82-8 103-65-1 108-67-8 98-06-6 95-63-6 135-98-8 99-87-6 104-51-8 91-20-3 1, 2, 3-T rich!oropropane Bromobenzene 2-Chlorotoluene 4-Chlorotoluene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 1, 2-Dibromo-3-Chloropropane 1, 2,4-T richlorobenzene Hexachlorobutadiene 1, 2,3-T richlorobenzene Methyl-tert-butyl ether Benzene T o!uene Ethyl benzene m,p-Xylenes a-Xylene Styrene lsopropylbenzene n-Propylbenzene 1,3, 5-T rimothylbenzene tert-Butylbenzene 1 ,2,4-Trimethy!benzene sec-Butylbenzene p-isopropyltoll1e1w n-Butylbenz.ene Naphthalene Other purgeables detected (up to l O highest peaks) NO VOLATILE ORGANIC COMPOUNDS DETECTED SY GC/ELCD/PID. ----- LAB NO. SUPERVISOR DATE ENTERED BY CHECKED BY - 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.75 5 2 - 5G1747 'J;i't 1 ~ -P= ~r./f.Y , r Derncted ug/L - u u u u u u u u u u u u u u u u u u u u u u u u lJ u u - I I I H D I I I I I I I I I I I I I I State of North Carolina Department of Environment, Health and Natural Resources Mooresville Regional Office .~;~· .a:·· ---~" DEHNR James B. Hunt, Jr., Governor Jonathan 8. Howes, Secretary Davidson Roofing Company Post Office Box 5602 DIVISION OF WATER QUALITY April 25, 1997 Statesville, North Carolina 28687 Attention: Chris Davidson Dear Mr. Davidson: RE: Well Water Sample Results Davidson Wells #1 & #2 173 Lauren Drive Well Former Elmore Well Iredell County, N.C. On April 7, 1997, staff from the Mooresville Regional Office of the North Carolina Division of Water Quality sampled the wells at the subject site. The samples were analyzed for volatile and semi-volatile organic compounds. Volatile organic compounds include a wide range of manmade compounds including, but not limited to, gasoline components and chlorinated solvents used as degreasers. Examples of semi-volatile compounds include some of the components of diesel, kerosene, and new and used motor oil. Laboratory results from these samples indicate at the time of sampling that volatile or semi-volatile organic compounds, which were tested\ for, were not present in your water supply. No further action will be taken by this office. ·• Should you have any questions, please call me at (704) 663- 1699, ext. 234. Enclosure: Lab Results Sincerely, ~ Paul R. Dahlen, P.G. Hydrogeologist L Iredell County Health Department \prd\davidson.wel 919 North Main Street. Mooresville, North Carolina 28115 Voice 704-663-1699 1-b:ffl Li J ?:j;,-&j FAX 704-663-6040 An Equal Opportunity/ Affirmative Action Employer 50% recycled/1()% post-consumer paper COUNTY QUAD NO fJ.• .. :. REPORT TO IIIRO Regional Ollice COLLF.CTOR(S): "u",c,~,,~.E~N~------ OA 1 E: 4f1197 TIME: PURPOSE: LAUOllATORY ANALYSIS 001))10 COD High HO COD Low JlS Coliform· MF fecal )1616 Colifo,m: MF 1'0111 }1504 IOC T urbility Residue , Suspended .SJO Total Suspended solids '" All..alinity lo pll 4 .S ,\llalinity to p1 I B.J C11bonatc llicarbonatc C11bon dio,idc Chlo1ide Chromium· llex 1012 Color: T,uc 80 C)·anidc 720 COIIIIIIENTS: l!!!!I -= == mgll. mg!L mg/I. 1100ml 1100ml mg/1 NIU mg/1. mglL uni1s llll!II. "'!!'I. mg/L mg/I. tn!!fl. mg/L ugl\. '" mg''- o,~ner· Location or Si1e· Uesc,iption of sampling point Sampling Method Rcmmks Diss. Solids 10100 F\uo,idc951 llardnc1s: to!al 900 I lardncss: (nou-ca,b) 902 rhcnoh l2lJO Specilic Cor,d, 95 Sulfate Sulfide 7U MBAS Oil and U1<,nsc Silica II"""' FmmnlJd,~J., NIUuN610 11':N 01 N 625 N02 •NOJ n, n 6JU r: T Ola I a, P 665 rm -liiiiiliil IH\'ISION OF WATEll QU,\LIT\' .,.I Chr111i,lt} l.•honlot·) ltrpn,t I t:rour,d W•tn Qu•lity s,v,lf>L~l'RIORI I y (DROUllNE □E~HCRUENCY BJ (·JIA1NOF("US10D\' @] SAMl'I.E-1 Yl'E IM\'lllSON \\"El.I. Ill mgll. mg/I. mgll. mgll. ug/1. t,~thos/cm2 mg/I. mg/L mg/I. m!VI. ,,,,,,1. n1;:1I. msJL n1gll. 1ui:1L n,gll. 11,51[. liiiilil liiii liiil □ 1\g·Sihc, 46566 AI-Alul!liuu,n 46557 As-An;c11ic 46551 lla•O:uium 46558 Ca-Calcium 4655.! Cd-Cadiurn 46559 Cr•Ch,omium 46560 Cu. Coppc, I 0-12 Fe• 10011 10-15 Ill'• Mc,cu,v Jtl)!KI K•l'lllassiuu, ,lh555 ~1g-~l;,1'11c1iu.,, 'l.!7 ~1n-/l.111n1_1anuc 1055 Na-Sodium 929 Ni-Nicl..cl l'b-1.caJ 4650-1 Sc·Scleniu1n '" Zir,c 46567 li!illiil - I.al, Number 7GU778 Date Rccci, ed 4/8197 Time Rccci,cd 9 00 ,\~1 Recci,ed Uy us Rdcn~cd Uy DS Date reporicd: .\12Jl'H ugll. {)1 !!anochh>1 inc l'csticiclcs uglL Organorhosphorus l'cstic1<lcs ugll. Nitro!!C" rcslicidcs ug/L mgll. Acid I lc,bicidn uglL ugiL \'. Semis ola1ilcs ugll. ug'L U!c(II. '"!'''· ongll. I rll-Oa,ulinc lt:.ngc "!!'I. I 1'11-1111:X (i11,ulmc lbn;:r 111gll. u!Ul. ugil. ugll. ugll. 'GOIIB M'O - ------ GROUNDWATER FIELD/LAB FORM Counly -,..,e,d,,_ l 1 Quad No l. (, 7,,-, Lal. 3s·• l/).',<;y 11/II Serial No·--~----- Long. f:u" _:;-7" ~ )' "' t J Heport To: Ano. Fn~ Hno. wano. Wino. SAMPLE PRIORITY Eg11ou IINE □icMEllGENCY 0c1 IAIN OF CUSTODY WSHO, l<inslon fO, Fed. Trusl, Cenlral 011., Oilier: _________ _ Shipped by: Bus,<Cotirli,,, Hand Del. Oiher· _____________ _ fl o I I h C a I o I I II n Depn1trne111 of E11vlrornnc111, llcnll/1, nntl Nriturnl ncsources IJIVISION or-EINlnotlMEIHAL MAIHIGEMEII r. onoutllJWAl En SECTIOII 0 Lab Nu111ber ___ 0 Dale neceivj,Ll__ .,:LI~ ,g_J__ Time 9 Jl1 ...... )~-- 11ec·d by:_~ Fro111: Ous,®r, llantJ Del.. 011,or: _________________ _ Dala E11lry Oy: ______ Ck: ______ _ Dale 11eporled: ______________ _ ~ / Pu, pose: Colleclor(s): ~ h Igo-Date y/115·7 Time // .' ~·j Uaselino, Cornplnint, Co111pliunce1 LUST, Pesticido Sludy, Federnl ·rrusl, OIiier: C..u ,L.,. -Jl ;•~ )_ L t1 "7\ • 1c11clo one) FIELD ANALYSE s e Owner J., ~-L.< J, 35'" -"'--'P'--'.'-.._:l'__,'-------------------------.. , --z/ I 7.> -pf-1400 -J-vspec. Cond.9, _ _,/~-al.25° C Localiorr or sile "«· '"- Temp.10 18 °c Odor Description of sa111pli11g poinl _;5.r.,,s~c:~i~c~•~.-l=--"=·l-d=gc~J~-------------------Appearance C(,, C, /c· c(~~6..,z Sa111pli11g Mellrod -~~------r.,c-=----.--------Sample lnlerval _______ _ ) r, -' ( (~p. b:ulo1, n1c) Field Analysis By: J ,; uc..,_ lle111arl<s ,: 1.,_, C .... ,~ (pumr,i11g ilinR,ili lemr,. etc) LABORATORY ANALYSES --BOD, 310 mg~! Uiss. Solids 70300 mq/1 Ag· Silver 465GG ugll Organochlo1ine Peslicides --COD High 340 mg/I Flourido 95 I 111q/l --Al -Aluminum 4G557 uq/1 Organophospho,us Peslicitles --COD Low 33S 111911 Haidness: l olal 900 ----n,q/1 As -A, senic 46551 uq!I Nil1ogen Pesticides Coliform: MF Fecal 31616 /100ml Hmdness jnon-cmb) 902 mq/1 Oa -Bmiu111 46550 ug!! --------Colilor111: MF Tolal 31504 1100ml Phenols 32730 ----ug!L Ca • Caldun1 46552 mqfl J\cid l-le1bicides --TOG 680 mql! .,Specific Cond. 95 utv1110s/c1112 Cd -Cadmium 46559 ug/1 ----.x Turbidily 76 NIU Sulfate 945 rnqtl Cr -Chro111iurn 4G5G0 ug~! Ser11ivolalile Orgr111ics ----Residue., Suspended 530 mg/I --Sulfide 745 mqll Cu -Copf~er 46562 uqll -------Fe-ho114G5GJ ug~ x ·------------·-··------. I-lg -Mc,curyJ 1900 ug/1_ Volnlilo 01um1ics (VOA bultl1.?) -------~H 403 uni If K -Polassiu111 4G555 rng/1 --·-------· ·----------·----/\lkali11ily to pl-I 4 .5 410 111911 _!v1q -Maq11csiu111 46554 lll~H' "!I'll -Gasoline nange --------Alkalinily lo pl·I 8.3 415 111911 Mn -Manganese '1G5G5 uq/1 ·1 Pl-I -□-I EX Gasoli,10 f1a11go --Carbonate 445 mgtl NH, as N 610 111q/l Na · Sodiu111 4G55G 1119!1 ---------- 1715) Bica, bona le 440 111911 --J KH.as.Ji . .£2' •ugtl.. --Ni -Nickel ugll --·carbon dioxide 405 mg/I NOe + NO as N 630 mq/l Pb -Lead 4G564 uqtl ----·--Chlmido 940 my/I P: Tola! as P 665 n1qll Se -Selenium uq(! Chromium: Hex 1032 ugll Zn -Zinc 4G567 uq/1 --Color: True 80 Pt-Co --Cyanide 720 mgll Lab Cornmenls: -------------------------------------~~------------------- -GW-54 nEV. 6'93 For Dissolved Analysis -sulrniil filtered sarnplc and w1ile "DIS" in bloclc ,· ·.··•: ,-.•. . : liiiliiiiil liiiiii iiiiii liiiiiil -----l!!!!!!!!!I I!!!!! I!!!!! i!!!!I == == liiiiiiiiiil - REPORTED BY CHECKED BY REVIEWED BY SAMPLE TYPE: 108-95-2 111-44-4 95-57-8 541-73-1 106-46-7 100-51-6 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 65-85-0 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 - 91-57-6 77.47.4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 208-96-8 -- WATER PHENOL 815(2-CHLOROETHYLI ETHER 2-CHLOROPHENOL 1,3-DtCHLOROBENZENE 1,4-DJCHLOROBENZENE BENZYL ALCOHOL 1,2-DICIILOROBENZENE 2-METHYL PHENOL 815!2-CHLOROISOPAOPYL) ETHER 4-METHYL PHENOL N-NITROS0-01-N-PAOPYLAMINE HEXACHLOROETHANE NlfROBENZENE ISOPHORONE 2-NITRO PHENOL 2,4-DIMETHYL PHENOL BENZOIC ACID 815{2-CIILOROETHOXY) ME THArJE 2,4-0ICHLORO PHENOL 1,2,4-TRICHLOROBENZENE NAPIHI\ALENE 4-CHLOROANILINE HEXACHLOROBUT ADIENE 4-CHLOA0-3-METHYL PHENOL 2-METHYL NAPHTHALEUE I-IEXACHLOROCYCLOPENT ADIENE 2,4,6-TRICHLORO PHENOL 2,4,5-TRlCHLORO PHENOL 2-CHLORO NAPHTHALENE 2-NITROANILINE DIMETHYL PH TH ALA TE ACENAPHTHYLENE - - - 10 10 10 10 10 20 10 10 10 10 10 10 10 10 10 10 50 10 10 10 10 20 10 20 10 10 10 10 10 50 10 10 - - EHNR/DWQ LABORATORY SEMI-VOLATILE ANALYTICAL REPORT ANALYSIS RESULTS u 99-09-2 u 83-32-9 u 51-28-5 u 100-02-7 u 132-64-9 u 121-14-2 u 84-66-2 u 7005-72-3 u 86-73-7 u 100-01-6 u 534-52-1 u 86-30-6 u 101-55-3 u 118-74-1 u 87-86-5 u 85-01-8 u 120-12-7 u 84-74-2 u 206-44-0 u 129-00-0 u B5-6B-7 u 91-94-1 u 56-55-3 u 218-01-9 u 117-81-7 u 117-84-0 u 205-99-2 u 207-08-9 u 50-32-8 u 193-39-5 u 53-70-3 u 191-24-2 - -11!!!!!!1 3-NITROANIUNE ACENAPHTHENE 2.4-0INITRO PHENOL 4-NITnO PHENOL DIBENZOFUAAN 2,4-01NITnOTOLUENE DIUHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANlllNE 4,6-DINITA0-2-METHYL PHENOL N-NITROSOOIPHENYLAMINE 4-BROMOPHENYL PHENYL ElHErl HEXACHLOAOBENZENE PEN f ACHLOAO PHENOL PHENANTHAENE ANTHRACENE 01-N-BU fYL PH TI IALATE FLUORANTIIENE PYRENE BU TYLDENZYL PIHi !ALA TE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE 815{2-Erl-lYLHEXYL) PI-ITHALAI E D1-N-OCTYL PH TH ALA TE BENZO(B)FLUOnANTHENE BENZOIKIFLUORANTHENE BENZOIA)PYRENE INDENO! 1 ,(-,3-CD)PYRENE 018ENZ0t A,H) AN Tl IRACENE BENZO(G,H,l)PEnYLENE !!!!!!!!I !!!!!!I l!!!!I LAB NO. 7G0778 SUPERVISOR--,::: f ./( DATE-::clf-''-c-'+.L.,L 10 u 50 u 10 u 50 u 50 u 10 u 10 u 10 u 10 u 10 u 50 u 50 u 10 u 10 u 10 u 50 u 10 u 10 u 10 u 10 u 10 u 10 u 20 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u !!!!!I I!!!! l!!!!!I 7 l!!!!!!I SEMIVOLATILE ORGANICS REPORT -DWQ LAB PAGE 2 NO BASE/NEUTRAL OR ACID EXTRACT ABLE ORGANICS DETECTED BY GC/MS. LAB NO. __ .:_7.=G.::0_:_7_:_7.::.8 TOL-Target Ouantitation limit-Subject to change due to inslrurnenl sensitivity T-Tentatively ldentilied, estimated concentration E-Estimated Value U-Samples analyzed for lhis compound but 1101 detected •N-Sample not analyzed lor this compound D-Detected below quantitation li111il H-Holding lime exceeded COMMENTS:--------------------------------------------------- :·: l!!!!!!!!!!I l!!!!!!I l!!!!!!!!!!I l!!!!!!!!!!I l!!!!!!!!!!I I!!!!!! l!!!!!!!I l!!!!!!!!!!I l!!!!!!!!!I I!!!!!!!!!! l!!!!!!!!!I l!!!!!!!I l!!!!!!!!!!!I !!!!!!!!!!I l!!!!!!!!!!I l!!!!!!!!!I l!!!!!!!!!!I l!!!!!!!!!I REPORlEO BY CHECKED BY REVIEWED BY SAMPLE TYPE: 75-35-4 75-09-2 156-60-5 75-34-3 590-20-7 155.59.4 67-66-3 74.97.5 71-55-6 563-56-6 56-23-5 107-06-2 79-01-6 76-67-5 75-27-4 74-95-3 10061-01-5 10061-02-6 79-00-5 127-16-4 142-26-9 124-48-1 106-93-4 108-90-7 630-20-6 75-25-2 79-34-5 TOL- T- E- LJ. N- 0- M- COMMENTS: -- WATER 1, 1-Dichloroelhene 0.75 Methylene Chloride 10 trans-1.2-Dichloroethene 0.75 1.1-Dichloroelhane 0.25 2.2-Dichloropropane 0.25 cis-1,2-Dicllloroethene 0.25 Chloroform 0.25 Bromochloromethane 0.75 1. 1, 1-T richloroe\hane 0.25 1. 1-Dichloropropene 0.25 Carbon Tetrachloride 0 75 1,2-Dichloroelhane 0 25 T richloroelhene 0.25 1,2-Dichloropropane 0.25 Bromodichlorornett1ane 0.25 Dibromornethane cis-1,3-0ichloropropene 0.25 lrans-1,3-0ichloropropene 0.25 1, 1,2-Trichloroethane 0.25 T etrachloroethene 0.25 1,3-Dichloropropane 0.25 Oibromochloromethane 0.75 1,2-Dibromoethane Chlorobenzene 0.25 1, 1, 1,2-Tet,achloroethane 0.25 Bromororm 0.5 1, 1,2,2-Tetrachloroethane 0.75 Targel Ouanli1ation Limit-Subjecl to change due lo instrument sensilivity l entatively Identified. not confirmed Eslimaled Value Samples analyzed for this compound but not detected Sample not analyzed for this compound Detected below quanlilation limit GC/MS Analysis perlormed - - 11!!!!!!!!1 l!!!!!!!I EHNRIDWQ LABORATORY VOLATILE ANALYTICAL REPORT ANALYSIS RES UL TS u 96-18-4 1,2,3-Tr ichloropropa11e u 108-66-1 Oro1nobenzc11e u 95.49.5 2-Chlorotoluene u 106-43-4 4-Chlorotoluene lJ 541-73-1 1.3-0icl1!orobenzene u 106-46-7 1,4-0ich!orobenzene u 95-50-1 1, 2-Dichlorobenzene u 96-12-6 1, 2-0ibromo-3-Chloropropane u 120-62-1 1. 2. 4-1 richlorobenzene u 67-66-3 f texachlorobuladiene u 67-61-6 1,2,3-Trichlorobenzene u 1634-04-4 Melhyl-tert-butyl etlier u 71-43-2 Benzene lJ 108-66-3 Toluene u 100-41-4 Elhyl benzene u 108-38-3 rn.p-Xyle11es u 95-47-6 a-Xylene u 100-42-5 Slyrene u 98-62-6 lsopropylbenzene u 103-65-1 n-Propylbenzene u 108-67-8 1,3,5-Trimethylbenzene u 98-06-6 tert-Bulylbenzene u 95-63-6 1, 2,4· Trimethylbenzene u 135-98-8 sec-Bulylbenzene u 99-87-6 p-lsopropylloluene u 104-51-8 n-Bulylbenzene u 91-20-3 Napl1\halene Gasoline Range Estimated Total Petroleum llydroca1bon Other purgeables de1ected (up to 1 O highest peaks) NO VOLA I ILE ORGANIC COMPOUNDS DETECTED BY GC/ELCOIPID. l!!!!!!!!!!!I l!!!!!!!!!!!I l!!!!!!!!I l!!!!!!I I!!!! !!!!!I LAB NO. 7G0778 SUPERVISOR~ DATE~ ENIEREDO~ DAI E~~-c4H/'c/0~/1El-77"'"' 0,25 u I u 0 25 u 0.25 u 0.25 u 0.25 u 0.25 u u 0.25 u 0 25 u 0.75 u 5 u u u u 2 u 1 u u u u u u u u u u u mg/L rng/L 0.25 N Detected ugll 11111111 : '.• · APR ?·.1 1997 COUNTY !REDELL QUAD NO: REPORT TO J\IRO COLLECTOR{S) DAIii.EN ==,_ _______ Regional Office DATE: 411('11 llME· PURrOSE· LA BORA TORY ANALYSIS DOD JIO COD lligh HO COD Low JH Colifo,m: MF Ftt11 ll616 Colifo,m· MFTotalJ1504 roe T"urbitity Ruiduc, Sus~ndcd SJO Total Sus~nd..d solids pll AILa1inity to pll 4.5 AILalinity lo pll l.J C11bonatc Bic11bon;i.te Cubon dio,.ide Chlo,idc Ch,omiurn: lie, 1012 Colo,: T1uc 110 C~llf\idc no cor.1r.1EN1S: == == mg/I. mgl\. mg/L 1100ml 1100ml mwl NIU "'1!''- rng/L units mgJL m111L mg1L mg;L mg/L n•l!IL ug1L '" mg•L == 0,u,cr l.uc111ion of Sile llc,criplion of 53m11li01g f>oinl Snmpling Method· Rcm~,L~ lliss Solids 70100 Fluoridc951 lb,dncss. tm3I 900 I IJrdr,en· (1,on-c11rb) 902 Phenols 32710 Specific Cond " Sulf3lc Sulfide 745 ~UJAS Oil 3nd GrcJ,c SilicJ Bomn l'o, maldch) de NIIJa,N610 I KN 35 N 625 NU2 !N0J ns n 610 I' ·101al n, I' fo(,S 1'0 l == == ·.!. ··' 1)1\'ISION OF \\',\TEH Qll,\UTY SM,!l'Ll:)'RLURITY E)ROUIJNf: Ot:Ml:RGl:N(·y EJ CIIAIN OF CUSl ODY @] SA"-11'LE ·1 Yl'E llA\'IIISON HOOFINI; WEI.I. Ii! n,gll mgll mgll mg1L ""'' ur-.1hos/cm2 mg/L mgll. mglL m!,1-ll. "'!.'-'I. "'!Ill. "'!.'-'l. m!')L mi:ll. mgil. mg•I. == == □ 1\g•Sihcr 465h6 Al-,\lu111in11m 46557 1\1-A,scnic 46551 lla•Il11riu111 46558 Ca•CJlcium 46552 Cd·CJdium 46550 C1-C!uou,iu1n 46S60 Cu• Copper I042 Fe-Iron 10~5 11!,I.· ~lc,curv 71'100 K•l'utnssi11n1 ~C,555 M)!'.• Magncsiu,n '127 ~ln-~1n11µm1c,e !USS Nn-Su<lium 92'1 Ni-NicLd l'b•l.end 4U5l,,I Sc·Selcniu,n /.uJ.inc 4b567 == == 1.~1, Nuu,t,,,, 11;077<, llJlc Rccci,cd ~/~197 I irnc Rttci-cd O 00 AM Rccci,cd llv DS Rclc~<cd lh llS D~lc ,cponcd : 4121,•)7 ugl(. U1ganod,!orinc l'esticidcs ugll. llr~311ophosphorus Pcstici<lcs 11!,l.il. Nitroi:en Pesticides ugll. mglL 1\ciJ lkrLicides U!,1-ll. ugll. ' Semi, olalilcs ugll. l l'H•Uicsd Range ugll u~IL ' \' olalile 0r~3nin ! \"(),\ l101tlc) n,;rrl. 111!','I. I l'IHfa~olin~ Raugc 111111. 11'1 I.IJ I EX (i11<1•h11c ltnn11~ n,g1l. u;,il. ug•I. 11~11. ug•I. ·,:;on&APfl == == == == == GROUNDWATER FIELD/LAB FORM Counly ~"" J, ,Cj Quad No L{,J h I Lat. 3.f"5'21 5-'J '' N Serial No. ______ _ P, G> --...., , ....., 1 11u Long.6 -' 1 \. T Report To: ARO, FRO,@, RflO, WaRO, WiRO, SAMPLE PRIORITY [BnoUTINE □EMERGENCY [i;ICHAIN OF CUSTODY WSRO, l(inston FO, Fed. Trusl, Cenlral 011., Oilier: ________ _ r~ o r I h Caro Ii II a Depa1tnrn11I of Environment, 1 lcallh, and Natural nesources OIV,ISION OF ENVIRONMEtHAL MAtlAGEMEtH-GROUNDWAlEFl SECTION 0 Lab Number _.:}Ci d..'.J '\ 'e Date Received L. -~ fl]_Tirne 9-W~-- llec'd by: __ D--'-"=-From: Bus~ Hand Del., Other: ________________ _ Data Entry By: ______ Ck: ______ _ Date neported: ______________ _ Shipped by: Bus~·Coun .r, I land Del., OIiier· '\ -:ii-Purpose: Collector(s): ~ Date 7,/ f] Time /) .' j5 Elaseline, Compla_inl, CornplianceJLIJST, Peslicide Sludy, Federal Trusl, 011,er: ~2. ;",. • c11clg one) FIELD ANALYSES .6 Owner vc~us/Jc= (""3'; LJ• \,1..t...1...-s2~----------------- pt-1,00 --'-.S'": 0 Spec. Cond.91 --'J'-'/'--a~° C Location or sile --------------------------------- Ternp.10 ----1A~~0 c Odor Descriptionolsa111plingpoi11t ¼2'zrr1 (,, ·J•r 0 j~l.J.------------------ Appeara11ce < 1,, ,(,c,;.t,vi,_,;,: Sarnpling Method --------~--=~ ____________ Sarnple l11terval ________ _ ~ bail111, 9lc) Field Analysis By: llernarl<s / ~ j n, ~ .) ._,, - LABORATORY ANALYSES BOU 310 1119/J Piss. Solids 70300 111q/l ~g · Silver 4G5GG uy! Q9~l1lori110 Pustidtlos -----·- COO High 340 mg/I Flowide 951 1119/I Al -Aluminum 46557 ugtl O1ganophospl101us Pesticides COO Low 33S mg/~ Hardness: Total 900 mg/I As• Arsenic 4G551 ugll Nilrogen Pesticides -- Coliform: MF Fecal 31616 1100ml Hardness {non-carb} 902 mg/I Da • Barium 46558 ug/1 Colilorm: MF Tolal 31504 1100ml Phenols 32730 --· uq/1 . Ca -Calcium 46552 mg/I Acid He1bicides TOC 680 mg!i ,§gecific Cond. 95 uMhos/cm2 Cd -Cadmium 46559 ugtl --~ Turbidily 76 NIU Sulfate 945 mq~I Cr · Cl110111iu111 4G5GO uq1l Ser1,ivolalile O1gar1ics Residue., Suspended 530 mg/I Sullide 745 rng/1 Cu -Coeeer 46562 ugtl Fe -hon 46563 ugtl ----x Hg -Me,cwy 71900 ugtl Volalilo O1ganics (VOA bollle) --pH 403 unit~ K -Potassium 46555 1119/I ------Alkalinily lo pH 4.5 410 mgtl -~9....:......fv.!~gnesium 46554 n1q{l TPH -Gasoline nange _______ ------Alkalinily lo pH 8.3 415 111911 Mn -Manganese 46565 ug/1 TPI I -Ell EX Gasoline llange ---- Ca,bonale 445 11,gtl !ill, as M 6IO 111gfL Na -Sodium 46556 mq{I ----· -- Bicarbonate 440 n,q/1 JJ,tl.as.N-62' ·nl)I!. Mi -Nickel ug/1 ------. I Ca,bon dioxide 405 111911 NOe,-±.NOa as N 630 mgiL Pb· Lead 46564 ug/1 ------V Chloride 940 mg/I P: Tolal as P 66S mqll Se -Selenium uq/1 ---- Chromium: Hex 1032 ug/1 --Z11 -Zinc 46567 uy/1 Color: True 80 Pl-Co ---- Cyanide 720 mg/I Lab Comments:----------------------------------------~-------------------- GW-54 lll:V. 6193 For Dissolved Analysis. submit lilleied sample and w1ile "DIS" in block. liiii!I I &Iii{ i;;;;;a a;;; == liililll' 11!111111 == == == == ~ EHNR/DWQ LABORATORY LAB NO. 7G0776 SEMI-VOLATILE ANALYTICAL REPORT -~ REPORTED BY SUPERVISOR . _. CHECKED BY DATE / 7 a - REVIEWED BY J?1Y ENTEREDB~ SAMPLE TYPE: WATER ANALYSIS RE SUL TS DATE \:. ,, .. l 62-53-3 ANILINE 10 u 606-20-2 2,6-DlNITROTOLUENE 10 u 108-95-2 PHENOL 10 u 99-09-2 3-NITROANILINE 50 u 111-44-4 81512-CHLOROETHYL) ETHER 10 u 83-32-9 ACENAPHTHENE 10 u 95-57-8 2-CHLOROPHENOL 10 u 51-28-5 2,4-DINITAO PHENOL 50 u 541-73-1 1,3-DICHLOROBENZENE 10 u 100-02-7 4-NITRO PHENOL 50 u 106-46-7 1,4-DICHLOROBENZENE 10 u 132-64-9 DIBENZOFURAN 10 u 100-51-6 BENZYL ALCOHOL 20 u 121-14-2 2,4-DINITAOTOLUENE 10 u 95-50-1 1,2-DICIILOROBENZENE 10 u 84-66-2 DIETHYL PHTHALATE 10 u 95-48-7 2-METHYL PHENOL 10 u 7005-72-3 4-CHLOROPHENYL PHENYL ETHER 10 u 10B-60-1 815(2-CHLOROISOPROPYL) ETHER 10 u B6-73-7 FLUOAENE 10 u 106-44-5 4-METHYL PHENOL 10 u 100-01-6 4-NI rROANlLINE 50 u 621-64-7 N-NITROSO-D1-N-PROPYLAMINE 10 u 534-52-1 4,6-DINITR0-2-METHYL PHENOL 50 u 67-72-1 flEXACHLOROETHANE 10 u 86-30-6 N-NlTROSODIPHENYLAMINE 10 u 98-95-3 NITAOBENZENE 10 u 101-55-3 4-BnOMOPHENYL PHENYL ETHER 10 u 78-59-1 ISOPHORONE 10 u 118-74-1 HEXACHLOAOBENZENE 10 u 88-75-5 2-NITAO PHENOL 10 u 87-86-5 PENTACHLORO PHENOL 50 u 105-67-9 2,4-DIMETHYL PHENOL 10 u 85-01-8 PHENANTHRENE 10 u 65-85-0 BENZOIC ACID 50 u 120-12-7 ANrl-lRACENE 10 u 111-91-1 BIS(2-CHLOROETHOXY) METHANE 10 u 84-74-2 Dl;N-BUTYL PH I HALA 1 E 10 u 120-83-2 2.4-0ICHLORO PHENOL 10 u 206-44-0 FLUORANTHENE 10 u 120-82-1 1,2,4-TRICHLOROBENZENE 10 u 129-00-0 PYRENE 10 u 91-20-3 NAPHTHALENE 10 u 85-68-7 BUTYLBENZYL PHTHALATE 10 u 106-47-8 4-CIILOl10ANILINE 20 u 91-94-1 3, 3 '-DICI ILOROBENZIDINE 20 u 87-68-3 llEXAC/lLOAOBU f ADIENE 10 u 56-55-3 BENZO(A)ANTHRACENE 10 u 59-50-7 4-CHLOR0-3-METHYL PHENOL 20 u 218-01-9 CHRYSENE 10 u 91-57-6 2-METHYL NAPHTHALENE 10 u 117-81-7 815(2-ETHYLHEXYL) PHTHALATE 10 u 77-47-4 H EXACI ILOROCYCLOPENT ADIENE 10 u 117-84-0 Dl-N-OCTYL PHTHALA TE 10 u 88-06-2 2,4,6-TRICHLORO PHENOL 10 u 205-99-2 BENZO(B)FLUOAANTHENE 10 u 95-95-4 2,4,5-TRICHLORO PHENOL 10 u 207-08-9 BENZOfK)FLUORANTHENE 10 u 91-58-7 2-CHLORO NAPHTHALENE 10 u 50-32-8 BENZO(A)PYRENE 10 u 88-74-4 2-f~llROANIUNE 50 u 193-39-5 INDENOf 1, f,3-CO)PYAENE 10 u 131-11-3 DIMETHYL PHTHALATE 10 u 53-70-3 DIBENZO{A,HJANHIRACENE 10 u 208-96-8 ACENAP!ITIIYLENE 10 u 191-24-2 BENZO{G,H,l)PEnYLENE 10 u . liiiiil liiiiiiil liiiiiil == == == == == - SEMIVOLATILE ORGANICS REPORT -DWQ LAB PAGE 2 LAB NO. 7G0776 NO BASE/NEUTRAL OR ACID EXTRACT ABLE ORGANICS DETECTED BY GC/MS. TOL-Target Ouantitation Limit-Subject to change due to_ instrument sensitivity T-Tentatively Identified, estimated concentration E-Estimated Value U-Samples analyzed for this compound but not detected N-Sample not analy2:ed for this compound D-Detected below quantitalion limit H-. Holding time exceeded COMMENTS, _______________________________________________ _ --1!!1!!11 --l!li'!!!!!I 11!!!!1!!1 l!!!!!!I -1!!!1!!!11!1 11!!!1!!1 ; REPORTED BY CHECKED BY REVIEWED BY SAMPLE TYPE: 75-35-4 75-09-2 156-60-5 75-34-3 590-20-7 156-59-4 67-66-3 74-97-5 71-55-6 563-58-6 56-23-5 107-06-2 79-01-6 78-87-5 75-27-4 74-95-3 10061-01-5 10061-02-6 79-00-5 127-18-4 142-28-9 124:48-1 106-93-4 108-90-7 630-20-6 75-25-2 79-34~5 TOL- T- E- U- N- 0- M- COMMENTS· l!!!!l!!!I -. 11!!11' WATER 1, 1-Dichloroethene 0 75 Methylene Chloride 10 lrans-1,2-Dichloroethene 0 75 1. 1-Dichloroethane 0.25 2. 2-DicI1loropropa11e 0.25 cis-1,2-Dichloroelhene 0.25 Chloroform 0 25 Bromochloromelhane 0.75 1.1, 1-Trichloroethane 0.25 1. 1-0ichloropropene 0.25 Carbon Te1rachloride 0.75 1, 2-Dichloroelhane 0.25 Trichloroethene 0.25 1,2-Dichloropropane 0.25 Bromodichloromethane 0 25 D1bromomelhane cis-1,3-Dichloropropene 0.25 lrans-1,3-Dichloropropene 0.25 1, 1,2-Trichloroelhane 0.25 Te!rachloroethene 0.25 1. 3-Dichloropropane 0.25 Dibromochloromelhane 0.75 1.2-Dibromoelhane 1 Chlorobenzene 0.25 1, 1, 1,2-letrachloroethane 0.25 Bromororm 05 1, 1,2,2-Tetractiloroethane -0.75 Target Ouanlilation Limit-Subject to change due lo instrument sensitivily T enlalive!y Identified, not confirmed Estimated Value Samples analyzed for this compound but not detected Sample not analyzed for this compound □elected below quantitation limit GCIMS Analysis performed 111!!1 1!!!111 EHNR/OWQ LABORATORY VOLATILE ANALYTICAL REPORT ANALYSIS RES UL TS u 96-18-4 u 108-86-1 u 95-49-8 u 1 OG-43-4 u 541-73-1 u 106-46-7 u 95-50-1 1.2.3-Trichloropropane Bromobenzene 2-Ct1lorotoluene 4-Ctiloro\oluene 1. 3-lJiclilorobenzerie 1,4-Dichlorobenzene 1,2-Dichlorobenzene u 96-12-8 1. 2-Dib,omo-3-Chloropropane u 120-82-1 1.2.4-·1 ricl1lorobenze1ie u 87-68-3 Hexachlorobu!adiene u 87-61-6 1.2.3-T richlorobenzene u 1634-04-4 Melhyl-tert-bulyl ether u 71-43-2 Benzene u 108-88-3 l oluene u 100-41-4 Ethyl benzene u 108-38-3 m,p-Xylenes u 95-47-6 a-Xylene u 100-42-5 Styrene u 98-82-8 lsopropylbenzene u 103-65-1 n-Propylbenzene u 108-67-8 1,3,5-Trimelhytbenzene u 98-06-6 lert-Bulylbenzene u 95-63-6 1,2,4-Trimethylbenzene u 135-98-8 sec-Butylbenzer1e u 99-87-6 p-isopropylloluene u 104-51-8 n-Butylbenzene u 91-20-3 Naphthalene Gasoline Range Est1maled Total Petroleum Hydrocarbon Other purgeables detected (up to 10 highest peaks) NO VOLA 1 ILE ORGANIC COMPOUNDS DETECTED BY GCIELCD/PID 1!!!!!!11 l!!!!!!I 1!!11!!!1 11!!!1!1 LAB NO. 7G0776 ENJERED DA 0 25 0 25 U.25 0 25 0.25 0.25 0.25 0.25 0.75 5 2 mg/L 0.25 l!l!!!I mg/L Detected ugll 111!!!!11 u u u u u u u u u u u u u u u u u u u u u u u u u u u N -- I I I I I I I I I I I I I I I I I I I . I State of North Carolina Department of Environment, Health and Natural Resources Mooresville Regional Office .SA James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary DEHNR DIVISION OF WATER QUALITY May 28, 1997 Davidson Roofing Company Post Office Box 5602 Statesville, North Carolina 28687 Attention: Chris Davidson ·near Mr. Davidson: RE: Health Risk Evaluation Davidson Residence Well Iredell County I have enclosed the health risk evaluation for the water sample taken from your well on April 7, 1997. If you have any questions, please call me at (704) 663-1699, ext. 234. E/closures fprd.\da.vidscn. hrc 919 North Main Street, Mooresville, North Carolina 28115 Voice 704-663-1699 Sincerely, ~}Qz__-- Paul R. Dahlen, P.G. Hydrogeologist FAX 704-663-6040 An Equal Opportunity/Affirmative Action Employer 50% recycled/10% post-consumer paper I I I I I I I I I I I I I I I I I NORTH CAROLINA DEPARTMENT OF ENVIRONMENT. HEALTH. AND NATURAL RESOURCES DIVISION OF EPIDEMIOLOGY OCCUPATIONAL AND ENVIRONMENTAL EPIDEMIOLOGY SECTION DRINKJNG WATER HEALTH RISK EVALUATION GENERAL 7 COUNTY _.........c.hc...✓_ddf __ ..,__~ LABORATORY# '/&-6 71J Based on these anal)'tical results. this water should be considered safe for nonnal usage. ( ) ( ) ( ) ( ) Chemical analysis did not show any contamination. Water should be resampled if odor or taste persists. The water should not be used for drinking or cooking purposes; avoid prolonged bathing/showering. Based on these analytical results. this water is highly contaminated and should not be used for drinking. cooking. or bathing'showering. The \aboratOry results are not conclusi\"e. please resample. PLEASE 11'DICA TE 01' LAB SHEET THAT IT IS A RESAMPLE A'iD PROVIDE PREVIOL'S SA'1PLE Nl'MBER(S). CO~IME1'TS: For further information. corytact Dr. Ken Rudo. Occupational and Environmental Epidemiology Section. (919) 715-6430. DEH'JR 389 I (5'96 I Occupational and En\'ironmentJ! Epidemiology Section (Re\'iew 5/99) COUNTY QUAD NO: lllEllELL REPORT TO _>01_R_O~ ________ Rogional Office COl.lECTOR(S) : ,oc•c•c•~L~ECN~------ DATE: ◄n/9' TIME· PURPOSE: LAIJORATOll\' ANALYSIS BOD llO mg.IL COD lligh 140 mg/l. COD Low JH mg/I. Coliform: MF Fecal 11616 /IUOml Colifo1m: MFlo111l1~04 /1001111 rue mg/I Tuibitit)' NIU Rniduc .• Su1pc:ndod HO mg/I. T 01.1\ SuSJM:ndod !I01id1 mg/L pll uniu Allalinity lo p\14 5 1111111. At1alinity 10 pll !.l 111i;II. C11bonatc m11IL 8ic11bon1te m111L C11bon dio1<idc mwL Chlo,ide "'l!'L Ch101,1ium lie, IOJ1 Ul!I(. Color: T1ue 110 '" Cyanide 720 msiL C01'11\IENTS: 1111!1 - Location 01 Sile: Oo,c,iplion ofnmpling pOinl Sampling Method Rcmo,l1 Din Solid1 70100 Fluoride 951 lfa,dnoss· total 900 I l11dno11' (non-ca,l,) 902 l'hcnoh 12730 Specific Cond " Sulfate Sulfide HS '-HUS Oil and Gic.ne S1hca !11>1<>11 l'u,malJch)JC NIil as N 610 IKNa1NbB ' N02 •NOl 11 n 610 I'· lu1aluru,5 1·0~ IH\'ISION OF \\'ATEll l)llAUT\' St\~!f'Lf...r..BKIB-1LX EJ1tUlJIINE EJ CIIAINOFCUSlODY Ej SAMPLE l YPE !Jllt!S 11,\\'U,SON HES. mt1IL myL m"L "'!1/L 1111,11. uMho'l/cm2 mg/L mt1IL rnll,IL mll,IL mi.JI. llll(IL <0.01 1111_1.ll. rug/I. 1.4 m1_1.ll. 0.04 111)!11. lll!,'IL -- □ Ag·S,hn 40566 Al•Aluminum 46SS7 A,-A,unic 46551 IL••IIB1im11 4655B Ca·Cnlcum1 465S2 Cd-CaJiurn 46559 (,.Chromium 46560 Cu-Copper L042 fe-loon 10~5 ' I lg• ~k,cury l 1900 K-l'ot:111ium 46555 ~II(• M:i1_1.11csiu111 •J~l ~111-~l;1n1_1.;111oc 1055 Na· SoJ,um ')~') Ni-Nidel l'l,-1.o:id 40501 Se·S~kmum Zn Zmc ~h5hl - N.C. Ob:YT. Otr 1:N.YlkO>H.tEN'f. liEALkl.i ()f NATUttAL lll~)URCI.S. UAY 14 1997 DlilSIQM er l,licW!lmll wmtail "811i1Ull lllllilAl tf1S1: l.~h Nu1111,._-, ll->lC RocotHJ lime Recci\ed Reccl\rd Uy Rcle~ By U~tc lrp0flod · ugl\. 0111:inochlorinc re,licidet /(;11777 418/91 900A~I IJS us SIIJ/91 ui;fl. 01~:ir,opho1phc11u1 PnhciJe1 u111L N,1,ui;en rc11icide1 u11JI. mll,II. Acid lle,l1iciJe1 ugl\. ui;Jl. Semi, ul:iuln ugl\. I rll-D1ucl Rani;e ugil. < 0.2 ugil. ' ,·01:i1ile Oq;:inin t\"O,\ l>uuleJ ms1l. 111µ/I. I l'l l-ti;1,.,1i11c llnnt(c u~•l. I I'll-II 11:.'< ti,.,"lin~ ltnn~c rn~•I. u~JI. ui;il. u~,L "!e''L ---11!!1!!1 ' . •-• ••--•••---••••--••--•--------•---•---•----••••••••••• ••--•-•-•i•---H•-•••••,~,-i--11-••c•~•;•~ 'i•1••1-;-; ••• •••••••• ••••••-••••---•••••-•••••• 1 GROUNDWATER FIELD/LAB FORM Uepn11111c111 ol Envho1une111, llcallh, nmJ Natural ncsourc:cs --• -\ -DIVISIOU or EllVJnONMEIHAL Ml\111\GEMEIH -GllOUtlUWIITEll SECTION ' Counly T /'12. <k,, l i Quad No '-(, 7 1--Serial No. ______ _ -a J I II • I C G •• ....., / ·-u ,, Lal. 3'> '--/ 01 tv Long. c·,u ·, 1 ,\L 1,) neporl To: 11no, Fno.~ nno, Wano, Wino, WSRO, l<inslon 1'0, l'ed. Trusl, Cenlral 011., Oilier: ________ _ Sl1ipped by: Bus,~-I-land Del., Oilier_· ___________ _ SAMPLE PRIORITY [Zjnou IINE QEMEllGENCY G2Jc11/\IN or: CUSTODY 0 Dala Enlry lly: ______ Ck: ____ _ Dale 11epmled: __________ _ Colleclor(s): ))cl,le c, Dale <z;,/-:;/2·2 FIELD ANALYSES 1," Prnpose: l inrn ~/~,/ __ .~J_u ___ Uaseline, C0111plai11I, Complinnce1 _I.US L Poslicido Sludy, Federal ·1,usl, Other: '\. j I cucl1 oroo) Owner __ (~b~--~, L•· ~v~c~L 1Q1~,~>·ci~k~,~~'~'-~""'~· ~•~ct.,,=~•~'------------------------ Location or sile s. & \ (J v ~-,-..u..<CJ."'-'--''-'--'1-'-"---,-----.-----,----~----,,--,----------- Descriptio11 of sa111p1i11g µoinl J a,,.,·\ l.\..--. oc ,d: _. t ? · ·.l.,:~·-~'-~·•~"~·~-~(_d=;~-'k~·--------- pl-l,00 -►.s Spec. Cond.94 __ "]~/_ al-25° C Temp.10 / J 0c Odor-----,----- 1\ppearance C!a,"c f_c.(,.,,.. G o·· Field Analysis By: j)a_D/: LABORATORY ANALYSES 1 J -' I ~ Sampling Method --------,5),iiiei.DiC•i --------Sa~11plo lnlerval ________ _ fle111a1ks vc, -, ;v,, >u·-;</ (pumping \lmt, ail limp. 1Lc) / BOD, 310 mg/I Diss. Solids 70300 m~I Ag. Silver 46566 ug/1 O1ua1mcl1lori11e l'eslicides COO High 340 mgll Flowide 951 m~I Al• /\lumiriu111 46557 UlJI\ --_9._1ganophospl101us Peslicides COD Low 335 rngJI Hardness: ·101al 9U0 111Y£L As• A1senic 46551 uq/1 Nitrngen Pesticides ----Coli101111: MF Fecal 31616 /1001111 Hmdness (non-carU) 902 111911 Ua • Oa1iu111 46558 uq/1 ----Colilornr: MF Total 31504 /1001111 ehenols 32730 ug1_ Ca• Calcium 40552 mq(I Acid Heibicides TOG 600 mg/I_ _§necilic Cond. 95 --uMl10s/cm~ Cd -Cadmium 46559 ug/1 --Tu1bidity 76 NTU Sulfate 945 lllq/1 Cr -Cluomium 4G5G0 --ugtl Semivolalile O1ganics nositluo., Suspomletl 530 111gtl --Sul/ido 745 mqtl --Cu -Copeer 4G5G2 uq~ Fe -hon 4G~63 ugtl --- ~ ----·· ~ I lg -Mercu,y 71900 uqtl Volalilo O1ya11ics (VOA bo\lle) --pl-I 403 units K -Polassiu111 46555 111y11 --Alkalinily to pl-I 4.5 410 mg/I _Mg_:__Maqr1esiu111 46554 mq/1 __!~t!._:_ Ga_:~line Range ------Alkali11ily lo pl-I 8.3 415 mytl -~~1a11ua11ose 4G5G5 uq~I I Pl I -U'I EX G.isolino llanuo ------Cmbonale 445 rngtl NI-I, asN GI0 rnq~!. Na -Sotliu111 4G556 rnq~I ------Bicmbonale 440 mg/I IJ,1'1...as_N_l;2s • 111)11 --J'JL.!1ickel ugll -I -- Cmbon dioxide 405 111911 ~ ' ii _NO~N~ as N 630 mgll.. Pb -Lead 4G56-4 ufl!.! ----Chloride 940 111u1! P: Toi.ii as P GGS 111qtl --So -Selenium uu/J V ----Ch10111iu111: I lex 1032 ugil Zn -Zinc 4GSG7 Uq/I Color: lJUe oo Pl-Co ' --Cyanide 720 mgtl Lab Commenls: ----------------------------------------;------------------------- GW-54 REV. 6193 for Dissolved Analysis -submit liltmed s.iruple ,mtl wdto '"UIS" in block. -- --------- - --- ---- El INRIOWQ LABORATORY LAB NO. 7G0777 c\~ VOLA llLE ANALYTICAL REPORT REPORTED BY SUPEHVISOR CHECKED BY DATE REVIEWED BY af!,,, SAMPLE TYPE: WATER ANALYSIS RESULTS 75-35-4 1, 1-0ichloroelhene 0.75 u 96-18-4 I. 2,3-T richloropropane 0.25 u 75-09-2 Methylene Chloride 10 u 106-66-1 Bromobenzene 1 u 156-60-5 trans-I. 2-Dichlmoelhene 0 75 ll 95-49-6 2-Chlorololuene 0,25 u 75-34-3 1, 1-0ichJoroethane 0.25 u 106-43-4 4-Clilorotoluene 0.25 u 590-20-7 2 ,2-Dichloropropane 0.25 u 541-73-1 1,3-Dichlorobenzene 0.25 u 156-59-4 cis-1,2-Dichlo1oe\hene 0.25 u 106-46-7 1.4-Dichlorobenzene 0.25 u 67-66-3 Chlorolorm 0.25 u 95-50-1 1.2-0ichlorobenzene 0.25 u 74-97-5 B,omochloromethane 0.75 u 96-12-6 1. 2-0ibromo-3-Chloropropane u 71-55-6 1, 1, 1-T richloroelhane 0.25 u 120-82-1 1.2,4-T,ichlorobenzene 0.25 u 563-56-6 1.1-Dichloropropene 0.25 u 67-66-3 I le~aclllorobuladiene 0 25 u 56-23-5 Carbon Tetrachloride 0.75 u 67-61-6 1.2.3-T 1icl1lo1obenzene 0 75 u 107-06-2 1,2-Dichloroethane 0.25 u 1634-04-4 Melhyl-lert-bulyl ether 5 u 79-01-6 T1ichloroethene 0.25 u 71-43-2 Benzeue u 76-67-5 1.2-Dichlorop,opane 0.25 lJ 108-86-3 loluenc u 75-27-4 Brornodichlorornetllane 0 25 u 100-41-4 Ethyl benze11e 1 u 74-95-3 Oibromomethane u 106-38-3 m,p-Xylenes 2 u 10061-01-5 cis-1,3-Dichloropropene 0 25 u 95-47-6 a-Xylene u 10061-02-6 h ans-1,3-0ichloropropene 0.25 u 100-42-5 Styrene u 79-00-5 1.1.2-T1ichloroetha11e 0.25 ll 9B-62-B lsop1opylbc11zcne lJ 127-18-4 ·1 etracllloroeltic110 0 25 ll 10:J-65-1 r1-l 'ropylber,zm10 ll 142-28-9 1. 3-0icl1loropropa110 0.25 ll 108-61-8 1.3,5-1 rimelhylbonzerm I) 124-48-1 Oib10111ocllloronmll1m1e 0,75 ll 98-06-6 ler t-llutyllic11ze11e u 106-93-4 1.2-D1b1ornoc\l,a1w ll 9(;.GJ-G I ,2.4-l 1i111etl1~llmtlll!IIU I) 108-90-7 Cl1torobenze11e O 25 u 135-98-8 scc-llutylbc11zer10 u 630-20-6 1. 1.1.2-1 ol,ochloroolhano 0.25 ll 09-87-6 p-isopro11yltulucno ll 75-25-2 B1ornolmrn 0.5 ll 104-51-6 n-Bulylbenzer1e u 79-34-5 1. 1,2,2-I etrachlomethane 0.75 u 91-20-3 Uapl1\11alc11e u mull. mull TOL· l arget Ouantilation Limit-Subject lo Gasoline Hange Estimated l otal Petroleum Hydroca1bo11 0.25 N change due lo i11sln1111011l suns1fr;ily T-I cmlalivoly ldon1illod. not ccmlumcd 01hcr pur11calllus delm:lod Dutuclcd E-Estnnalcd Value (up lo to highusl peaks) uull U-Samplus analyzed lor this compound IJUI not cJetcc.:tud N-Sample nol analyzed for this compound NO VOLA I ILE OHGAt~IC COMPOUNDS D-Detected below quanlitation limit OE I EC I ED UY GCIEI.CDll'ID. M-GCIMS Analysis pc,lorrned COMMENIS: ---- --------- - 111!!1 11!!!!1 - I I I I I I I I I REFERENCE 20 I I I I I I I . I I I I I I I I I I I I I I I I I I I I State of North Carolina Jame• •· Bunt, Jr., Governor Rhonda Morgan Route 14, Box 356 Mooresville Regional Office March 25, 1993 Statesville, North Carolina 28677 Dear Ms. Morgan: Subject: Well Sampling Results Morgan Residence Triple AAA Septic Iredell County, N.C. Ref. 20 On February 22, 1993, I sampled your well for nitrates/nitrites and fecal coliform. The results indicate that nitrates and nitrites are present at levels (11 mg/1) just above the 10 mg/1 groundwater standard. The level found should not be harmful to adults, however, children under one year of age should not drink it. I will forward you a health risk assessment report once I receive it. If you have any questions, please call me at (704) 663-1699, ext. 235. Sincerely, (!L;(}f:t(_ Chris DeRoller Hydrogeologist cc: Iredell County Health Department Laurie Martin, Hazardous Waste Section Julian Foscue, Solid Waste Section CMD/sc PO. Bo, 950, 919 North M.ln Sa=. 1'Aoo""'11k, NC l8115-09l0 • Telephone 704-653-1699 • FAX 704-66}-(,I)<() tv, E,iu.l Oppommity Affinran"' Action Emp>,c,,.,· I I I ! co~ :!!llir.° ---~c:~ -1pa1 vuAO t,u. -. L.;:LL_ S E fl l A L NO . LA l. LONG. -_, 1-dl-llil--~•M=--~~~L-nto v1ro nt,1 11,, __ \/atL._ .. =ies ___ ;es ;i_;;r:::1cl2 -,. ,..._ Division ol Environme !al MananemAnt DATE RECEIVEt1_· -· >-) Time -( · ( ,C':; " II, 'CC m:rr. OF NATURAL 1DS Groundwater Field/Lab ForllllESOURCES A"D Rec'd by: '· From: Bu~ - Re por I lo: A/1O, rn~J-nRci. WaRO, WiAO, SAMPLfu PRIORITY · MAR 1 1993 DATA rnrnv ev:_i:::)_H __ cK/41(/(/ , )Alf./: 1}R" C! JSTQ:f~l(u,-;in-IGE''.. Other \\'SRO, Klnslon FO Olhor _________ _ Shitiped by: Ous~ 01hor _______ _ [(] ROUTINE O EIAERGENCY OAlE REPORlED: __ J_/_J'_/_c_/_J ______ _ COLLEClOll[SJ: Q,,2-,/({( DAlE ,.?_(2.<(7'.1 TIME PunrosE: llml\:K Qf UIVIR!n~E,1'.t k -~1 B A8()l)R[S\1U[C(!M~li/l~ 1 !)ff IC Ee o -,pu MJ c E. LUST, OlHER FIELD ANALYSES DH-400 ____ Spec. Cond.g-4 ___ al 25°C Tomn.10 ____ .0 c Odor _______ _ Appoaranco ______ _ Taslo ______ _ rleld Analysis By: ___________ _ LA0OflAI011Y ANALYSES eoo!> J" motl coo High J" mg/I coo Low "' mg/I X. Colltorm:UF r • C •f J!618 <.... I / I 00ml Colllo1m:ur lo 11 l J 1 !.04 /100ml IQC ... mo/I T,ubldlt1 " NIU oH •OJ uni t1 -"tk • ti nl 11 lo oH '-' .,. mo/I AH ollnliy " "" •. J .. ' ,., D /I C1rbc,n111 "' mg/I Olc.,t,c,n111 ... mo/I Ar,onlc:1 ol•I I 00 1 "'" c .. t-on dJod,:h .. , moll X. Ch!nrldo ... mg/1 Ch!omlv<n:H11 1031 ug II ColtH:lruoo '" Pl-Co t: Io nl C • "0 .., D fl circle on-e) · Ow nor I IJl'II ,--A,1 _:;,_-_;(. 5{ c; j-rJ o; I r· ,· \i J;,,·,c_ Loe a lion s1 le . '( L.? £ ./ /7::) p C ,":~ /c..1QL,,; o, ! ' Oo:;crlpl/on o/ sampl Ing polnl /c•f' c-1l I~·,// Sarnnlir.p Method Remarks (pump, baller, olc".) tf/1fc1 £< .5(n"nf{ t,o-1 /J(f\tc!l-r r). I or ... Solld1 IOJOO mg/I Ag Sllur 1071 rluorl<,. "I moll Al 1'1umlnum I I 05 H•1dn1u:To11I ,., mg/I e, Bulum ·1001 Ha,dn••• (non·tlrb) '" mo/I c, c,rctum "' f>h1nol1 ]17 30 "'" Cd Cadmium I 02 7 Sp1clllc: Cond . " uUho1/cm1 Ch1omlum:To11l 103-4 Sutf I I• ,., molt c" Copp■r 1042 Sullld1 '" moll F • Iron 10H "' U1,cur7 T 11'00 " Pol1nlum '" "' U • gn1 11 um "' "". U1ng1n111 IO~ 6 "' Sodium "' NH3 .. " "• C),\:i) moll "' NI c ~ 1 I 1061 TKN .. N ti 15 mo/I '" l•td IO~ I N01 1 N03 "H 6JO I\. mg// s, S1l1n!um 1141 P;lol ■I 11 P 665· molt lo 11 nc 1091 --<:" .• <-r~~:: Sa mp I e In I e, v e I -~~'-"~----------- (pumping tlmo. air lornp, elc.} uoll 01g1nochlodn1 P'111lcld11 ug/1 o,g1nopho1phoru1 P'1tlfold11 "'" mg/I Acid H11dlcld11 vg/1 uc/1 8 ••• / ,..,ulfll £1111c1tbl1 o,,."'r,, \10 fl A.cld [1lr1cl1bl1 Or;1nlo1 ug /I uc/1 Purc11t1r, Org1nlC1 {VO~ borll,J mg/I . m<>'• '. 1 • 01brorno1lh1n1 1£0!1] ug II mg/I von ug II uoll ug ,r Lab Comments: OIV-S.. nEV. ll.'W For Dtssotved Analysls • subrnll l!ttorod tamplo and wrilo -·-··>·In block VlhNe Copy -Ornundwalor Conlral Ollle-0 Yollow Cor> · .,Qlonal Ollk:e Pink Cory, Conl,al Fl~• GnHclnm<i r.nnv. I Ph I I I •-: I I I I I I I I I I I I DEHNR MOORESVILLE R 0 State of North Carolina Department of Environment, . Health and Natural Resources Mooresville Regionol Office James B. Hunt. Jr., Governor Jonathan B, Howes. Secretary Dec 5 '96 12:56 P.10 E;J\ ----!~-- DEHNR DIVISION OF WATER QUALITY October 8, 1996 Rachel Brown 183 Lauren Drive Statesville, North Carolina 28677 Dear Ms. Brown: RE: Well Sample Results Iredall County I am sending you these sample results along with the State Toxicologist's health risk assessment for the water samples collected from your well on March 15, 1995 and February 7, 1996. As you can see, Dr, Rudo had recommended at that time that your well water not be used for drinking or cooking purposes, and that prolonged bathing and showering should be avoided. I will forward results of the samples I collected yesterday when I receive them. If you have any questions, please call me at (704) 663-1699, ext. 234. Enclosures ~rown.lt:r 919 North Main Street. Mooresville, North Corollno 26115 Voice 704-663-1699 Sincerely, Paul R, Dahlen, P.G. Hydrogeologist FN< 7D4-M3-6040 An Equol Opportunity/ Affirmotlve Action Employer 50% recycled/1~ pest-consume< paper I I I I I I I I I I I I I I 1· I DEHNR MOORESVILLE R 0 Dec 5 '96 12:56 P.11 State of North Carolina Department or Environment, Health and Natural Resources Mooresville Regional Office AW ... ~ __ ... James B. Hunt, Jr., Governor Jonathan 8, Howes, Secretary DEHNR Linda Diane Long, Regional Manager Florence Russell Route 14, Box 356 DIVISIOU OF EtNIROUMENTA~ MANAGEMENT May 2, 1995 stacesville, North Carolina 28677 RE: Health Risk Assessment Florence Russell Well Iredell County, N.C. Dear Mrs. Russell: Please find attached a copy of the Health Risk Assessment performed by Dr. Ken Rudo on·your well located at Route 14, Box 356, Statesville in Iredell County. If you contact Dr, ext. 243. KDW/sc Attachment should have any questions, please do not hesitate to Rudo at (919) 733-3410 or me at (704) 663-1699, Sincerely, ;J , ~ >f ✓h1:::-or1 Karen Walker v'f'[7 1 Hydrogeologist cc: Iredell County Heal.th Dep<l.rtment Ql Q North Moin Sheet. MooresviLie. North Corolina 28115 Telephone 704-663· 1699 FAX 704-663--6040 An Ec,uoJ Oooorturuty Affirmative Action Employer 50o/. recycled/ lO'l, post-consumer pape, I I I I I I I I I I I I I I I I 'I I I I I DEHNR MOORESVILLE R 0 Dec 5 '96 12:55 P. 12 N.C DE,l'T. OF ENVIRONMENT, HF, •. - ll"rlh car,,Hna O.paru.nt of l!.nviro,,,,..nt, Haal th, , Natural Rollib~ 11.n:s· · Division of lpiduuoloqy !nvironmentnl lpidemloloqy &action APR 26 1~~" Dri.nltinO Water Boll.1th IUllk :Val.U&ticn . I Cf EllY!P.GK~ElllAL KA'. .. I ca.neral TAlllSllll~ lfl1'1. • ......... ........, __,,,.., S?;-J<$t .......,..,..,,, ........ ......., -------- ( ) .... d on the ■-analytical naulta, thl.a vatar ahculi! ha c,onai.Su•ed aafa for normal u1a;e. (/:auc&l a.naly11• did not abow any eontw.nat1on. i:ratu ahould be ~••lll!i>l•d 1f ~= or ta■ta paruiata. I Th• water aho~ld not be usa6 for dr1nkinq or cook.in; pun:,os•s, pei4 prolongad l:>at.hin;/lhow•rinq. ) Jle■aO on th••• analytical raault•, thi• water i• highly contuiin■taO and ■h=ld not l:>e uaaa for driMini, cookinq or bat.hinq/ahowarinq, ( ) Tha laboratory raault■ are not conclusive, pleua ro■ample: PLEASE 'INDICATE ON LU S!!UT THAT IT IS AU~ AND~ PUVIOUS SAMPLE NUMBER I s) • COHMENTS: Tor furthar infor,oetion, contact ~r. Kan lh,do or Dr, Luann• Willi=-, b>viror=-ntal !tpiduuol~ Saetion, (919) 733-3410. O!ltmt 38'31 (5/92) l!.nvironmental Rpi~a,niol09Y S•ction (Review 5/95) - ---- --- - --- - - l!!!!!!ll l!!!!!!!I I!!!!!! l!l!l!!I I North Carolln ■ Department of Environment, Heallh, and Natural Resource! DIVISION OF ENVIRONMENTAL MANAGEMENT· GROUNDWATER SECTION I Counly __ 'I_,_e_c~l_e._l_l ----------- Quad No Uo1,.., -1$ Serial No. _____ _ 35° 1./;)' 58 1 ' L Bo· 5l.'18 11 Lal.-==--'-''-=-~-ong. ~-~-~~-~--- Report To: ARO, FRO,@RRO, WaRO, WiRO, 'i SAMPLE PRIORITY ~ROUTINE □EMERGENCY @CHAIN OF CUSTODY WSRO, Kinslon FO, Fed: Trust, Central Ott., Other: ________ _ Shipped by: B_us, ~Hand Del., Other_· ___________ _ 0 PurJX>se: · Collector(s): k Wo....l I"--"-1 · Dale 3 -lo -'I'S Time \;;:,: "0 P'"' Baseline, Complain!, Compliance, LUST, Poslicido Sludy, Fedor al Trusl, Other: 1'01\ L<,-Kva 11ooil,,cir;) 1atle or-..) FIELD ANALYSES Owner \:"\ b(<Zn C..f 'KLQSe..\l ( p,1--,0,-,do.... Mor::sc-c, vJ,..g • ~ C,w T~<-1~~~ --s·,<,:00s at 25° C Localion or sile 6o:i4:t-IL\ 6ox 3S<, , 5\;::d-e:sL?i ii e Ne. :z,1 \o:J7 l,, ,0 Spec. Cond... .------: :..;;;---° C Odor f\.DA.JL oH 400 Temp.10 l\ppearance_.....,,,,,.,,,c_ __________ _ Description ol sampling poir,1 'ls,l:d'.Ju, S,n k Spif:j?t Sampling Melhod ,P...,'-"c0.'"':..,.,:>'c.._ _______ ~--------Sample tnterval_.,al.,t.,Rl===-=•-=vfr'-"-'-- < _ d r, ,~.b..-1,MC) ';j" < • Cield Analysis By: .h~l,,,&1--L=~\~CJlA.~--------Remarks ..:,ub('\e o..-,-+s,C pc,u-,o\""l .:, ""'' oS --T" \ p.,n,:,r,g --... -.mp_.-.:.) L.ABORA TORY ANALYSES BOD, 310 ma/ Diss. Solids 70300 mg!I Aa • Silver 46566 uall Ornanochknine Pesticides COD High 340 mg,1 Flouride 951 rna/1 Al -Aluminum ◄6557 uni! Organophosphorue Pesticides COD Low 335 me,/ ~erQoe~~· TQ)gl 2QQ m!:!!1 As• Arsenic 46561 U"' Nitrnoen Pesticides Coliform: MF Focal 31616 1100ml Hardness (non-carbl 902 ma/I Ba -Barium 46558 U"' Colilorm: MF Tolal 3150◄ 1100ml ~b~nol~ ~~Z~Q ~g'! Ca -Calcium ◄6552 mnl Acid Herbicides TOC 680 .....,, Soocilic Coad, 95 --uMhos/cm2 Cd -Cadmium ◄6559 U"' T urbidily 7B NTU Sullato 9◄5 =" Cr -Chromium 46560 uni! Semivolatile Oroanics Residue., Suspended 530 mg,1 Sullido 7 ◄5 =" Cu -Co~r ◄6562 uni! Fe -Iron 46563 uni! >< Ha -Morcurv 71900 5-:? ua/1 '>< Volatile Organics (VOA bol11o) pH ◄OJ unit: K -Potassium 46555 mall Alkalinity lo pH 4.5 ◄10 rnglf Ma -Maanosium 4655◄ ma/ TPH -Gasoline Range I un" TPH -BTEX Gasoline Ranqe Alkalinily to pH 8.3 ◄15 mg,1 Mn -Mal"Klanese 46565 Carbonate 445 . mg,1 NH as N 610 o,Oq mn/1 Na -Sodium 46556 mall _ ----PT. OF Bicarbonate 4-40 mol Il:S~ as t,j ·fi25 mg/I "' -'"-' -· --""' • _·. ,dt,NT, rtr_,,n...,-::::", ... Cmbon dioxide 405 mall .x NO + NO as N 630 9.t.\ =II Pb · Load 4656◄ U"' 1:l .... 1r,.'fURA.L~'-n Chloride 9-tO mall P: Tolal as P 665 =" So -Selenium un" \ I ---U"' I / t.PR 1 ~ " I Chromium: Hex 1032 ua/1 Zn -Zinc 46567 I Color: True BO Pl-Co 'J Cyanide 720 mg,1 ...... on,~[¾\\l \'.1,1\1,c"•"' _, ""'" I\H.t-.L-lJl ,., Lab Comments: ----------------------------------------------"~-c:u: __ ,. __ ,1_1l_ll_Rl_G1_u ____ _ For Dissolved Analysis -submit filtered sample.and write "DIS" in b --' REPORTED BY CHECKED BY REVIEWED BY SAMPLE TYPE: 75.35.4 75-09-2 1 56-60-5 75034.3 590-20-7 156-59·4 67-66-3 74.97.5 71-55-6 563-58-6 56-23-5 107-06-2 79-01-6 78-87-5 75-27-4 74.95.3 10061-01·5 10061-02-6 79-00-5 127-18·4 142-28-9 124-48-1 1 06-93-4 108-90-7 630-20-6 75-25-2 79.34.5 TQL- T- E- U- N- D- M· COMI/ ·s, ----- WATER 1, 1-Dichloroelhene 0.75 Methylene Chloride 10 trans-1,2-Dichloroethene 0.75 1, 1-Dichloroethane 0.25 2, 2-Dichloropropane 0.25 cis-1,2-Dichloroethene 0.25 Chloroform 0.25 Bromochloromethane 0.75 1, 1, 1-Trichloroothane 0.25 1, 1-Dichloropropene 0.25 Carbon Tetrachloride 0.75 1,2-Dichloroethane 0.25 Trichtoroethene 0.25 1,2-Dichloropropane 0.25 Bromodichloromethane 0.25 Dibromomethane 1 cis-~ ,3-Dichloropropene 0.25 trans-1, 3-Dichloropropene 0.25 1, 1,2-Trichloroethane 0.25 T etrachloroethene 0.25 1,3-0ichloropropane 0.25 Dibromochloromethane 0. 75 1,2-Dibrornoethane Chlorobenzene 0.25 1, 1, 1,2-Tetrachloroethane 0.25 Bromoform 0.5 1, 1 ,2,2-Tetrachloroethane 0. 75 Target Ouantitation Limit-Subject to change due to instrument sensitivity Tentatively ldontifiod, not confirmed Estimated Value Samples analyzed for this compound but not detected Sample not analyzed for this compound Detected below quantitation limit GC/MS Analysis performed - - ---- - EHNA/DEM LABORATORY VOLATILE ANALYTICAL REPORT ANALYSIS RESULTS u 96-18-4 1, 2, 3-Trichloropropane u 108-86-1 Bromobenzene u 95-49-8 2-Chlorotoluene 0.72 106-43-4 4-Chlorotoluene u 541-73-1 1,3-0ichlorobenzene 0.43 106-46-7 1,4-Dichlorobenzone u 95-60-1 1,2-Dichlorobenzene u 96-12-8 1,2-Dibromo-3-Chloropropane u 120-82-1 1,2,4-Trichlorobenzene u 87-68-3 Hexachlorobutadiene u 87-61-6 1,2, 3-T richlorobenzene u 1634-04-4 Methyl-tart-butyl ether 0.27 71-43-2 Benzene u 108-88-3 Toluene u 100.41-4 Ethyl benzene u 108-38-3 m,p-Xylenes u 95,47-6 a-Xylene u 100-42-5 Styrene u 98-82-8 lsopropylbenzene u 103-65-1 n-Propylbenzene u 108-67-8 1, 3, 5-T rimethylbenzene u 98-06-6 tert-Butylbenzene u 95-63-6 1,2,4-Trimethylbenzene u 1 35-98-8 sec-Buty1benzene u 99-87-6 p-isopropyltoluene u 104·51-8 n-Butylbenzene u 91-20-3 Naphthalene Other purgeables detected (up to 10 highest peaks) FOUR UNIDENTIFIED PEAKS DETECTED BY GC/ELCD. ONE UNIDENTIFIED PEAK DETECTED BY GC/PID. -l!!!!!!.!!!I I!!!!!!! !!!!I . LAB NO. 5G306 SUPERVISOR DATE ENTERED BY CHECKED BY 0.26 0.26 0.25 0.25 0.25 0.25. 1 0.25 0.25 0.75 5 1 2 0.87 D D Detected ug/L u u u u u u u u u u u u u u u u u u u u u u u u ------------1!!!11!!1 l!!!!!!!!!I I!!!!!!!!! GROUNDWATER FIELD/LAB FORM CHAIN OF f'LJS"'TQrLV North Corollno \J LJL>fportment ol Environment, Health, end Nalurol Resources DIVISION bF ENVIRONMENTAL MANAGEMENT-GROUNDWATER SECTI_ON · T;lil.lb Number ~----;:, \ Ill \a _ SAMPLE PRIORITY Dale Rece,~)\ \ I \97 Tirn.':-(0 :q) __ E;::jROUTINE □EMERGENCY ·_. O·,·. _. _ Rec'd by: G From: Bus~ Hand Del, 52] Oilier: -------,=oc-------+.-~~,._----- ~--"'--CH/\IN OF CUSTODY --r:; · (,,7-:: :eport To: ARO, FR~F:9) RRO, WaRO, WiRO, 0.?la Entry By: / /; c-~ Ck: !s;C__~ ! __ _ /SRO, Kinston FO, Fed. Trust, Central Off., Other: ____ ~-----f)°(ile Reported / J J .,.., ,9(c ounly -Y..'lfcU.U Iuad No U//n-6 Serial No ________ _ a1. _:~_:,,_s_o_,~J~J_,~:>_-~B_'_1_ Long. f.-0~ 56 / hipped by: Bus,~~'Hand Del., Otl1er_· ____________ Purpoc.o: G tc' 1,-c 11 -'l'I J .-) :ollector(s):tj'C Cnci c ./( Date ID· IO .q5 Time 11: 35 A ,'>7 Baselino, Complain!, Compliance( LUST. Pesticide Study, Federal Trust, Other· j!,'.t:lcch en h,:,u It-, N'. _ c"cl,io.-..) -:1 'IELO ANALYSES owner H0,·,0 n.,u_.. !Zu_3"'"cLL 1-1,00 l,./.J ·ernp.10 lfa .. -S Spec. Cond.94 tt/{i,,,,hcs at~° C °C Odor noi1e Location or site &c«-t'-i·/ 1 L~0>< . 3-5 (c, :SbJ-w ,_;, f I, , 1-1 c 'L 'i L· · 1 -, Description of sampling point hnc 6 ",1-,p, 1.<.Ji lC h.c ,u:,( ,ppearance_J...J--"":1-'7 ___________ _ ·ield Analysis By: ~k=C~o~o~n~e~t_r _______ _ Sampling Method ~'~"'~L~•"'-,<-·"-----~~~~~-------Sample lnlerval-'-'~L-"''""1,..,,._i' ____ _ < -_ ( I jPurnp, b-1,~r. a1c) 11 ( ~ / c- RemarkS ~f-}t?C (). ,~~~r~-~-+-;::'=o··=·'=-=-'-=-==-=j•'-~7~'~·=----~---~------ l) ---I (pumpin<;i nme. u C•mp. •1c) l\..El..ORATORY ANALYSES BOD. 310 mall Diss. Solids 70300 mq/1 ~ -Silver 46566 ug/I Organochlorine Pesticides -- COO High 340 mg/I Flouride 951 mall A! -Aluminum 46557 Ug/I Organophosphorus Pesticides COD Low 335 mall Hardness: Total 900 mqll As -Arsenic 46551 ug/I Nitrogen Pesticides -- Coliform: MF Fecal 31616 1100ml Hardness (non-carb) 902 mall Ba -Oariurn 46558 ucj/I Coliform: MF Total 31504 1100ml Phenols 32730 ugil Ca -Calcium 46552 mcVI Acid Herbicides TOC 680 ma,I Specific Cond 95 uMhos/crn2 Cd -Cadmium 46559 uq/1 f-- Turbidity 76 NTU Sulfate 945 mall Cr -Chromium 46560 ug~ Sernivolati!o Orgc1nics -- Residue., Suspended 530 mg/I Sulfide 745 mall Cu -Coooer 4G562 ugll 1-x Fo • Iron 4G56J ug!.!_ Hg -Mercury 71900 \ l.j ugl__l_ :;,< Volatile Organics (VOA boltle) •-~ pH 403 unit:: K. Potassium 4G555 rngJI - lllkalinily to pH 4.5 410 mgll Mo -Maonosium 46554 mq/1 TPH -Gasoline Range Alkalinity to pH 8.3 415 mg/I Mn -Manganese 46565 U!J!I TPH -BTEX Gasoline nango Carbonate 445 mg/I NH as N 610 o.o s rnn1I Na -Sodiurn 46556 mq~I - Bicarbonale 440 =II I T}{I\I ....... N C'"JC -~II Ni -Nickel ug/I I Carbon dioxide 405 mq/I ·-x NO~ + NOa as N 630 J>:G m~! Pb -Lead 46564 uq/I // Chloride 940 mg/I P: Total as P 665 n1_9[]_ Se -Selenium ug/I V Chromium: Hex 1032 uq/I Zn -Zinc 46567 uq(I Color: True 80 --Pt-Co Cyanide 720 mg/I --REPORTED BY CHECKED BY REVIEWED BY SAMPLE TYPE: 75-35-4 75-09-2 1 56-60-5 75-34-3 590-20-7 156-59-4 67-66-3 74-97-5 71-55-6 563-58-6 56-23-5 107-06-2 79-01-6 78-87-5 75-27-4 74-95-3 10061-01-5 1 0061-02-6 79-00-5 127-18-4 142-28-9 1 24-48-1 106-93-4 1 08-90-7 630-20-6 75-25-2 79-34-5 TOL- T- E- U- N- 0- M- COMMENTS: ' -- - WATER 1, 1-Dichloroethene 0.75 Methylene Chloride 10 trans-1,2-Dichloroethene 0. 75 1, 1-Dichloroethane 0.25 2,2-Dichloropropane 0.25 cis-1,2-Dichloroethone 0.25 Chloroform 0_25 Bro rno chloromethane 0.75 1, 1, 1-Trichloroethane 0.25 1, 1-Dichtoropropene 0.25 Carbon Tetrachloride 0.75 1,2-Dichloroethane 0.25 Trichloroethene 0.25 1,2-Dichloropropane 0.25 Bromodichloromethane 0.25 Dibromomethane cis-1,3-Dichloropropene 0.25 trans-1, 3-Dichloropropene 0.25 1, 1, 2-Trichloroethan~ 0.25 T etrachloroethene 0.25 1,3-Dichloropropane 0.25 Dibro mochlo romet hane 0.75 1,2-Dibromoethano Chlorobenz:ene 0.25 1, 1, 1,2-Tetrachloroethane 0.25 Bromoform 0.5 1, 1,2,2-Tetrachloroethane 0.75 Target Ouantitation Limit-Subject to change due to instrument sensitivity Tentatively Identified, not confirmed Estimated Value Samples analyzed for this compound but not detected Sample not analyzed for this compound Detected below quantitation limit GC/MS Analysis performed -- -EHNR/DEM. L, ,dORATORY VOLATILE ANALYTICAL REPORT ANALYSIS RES UL TS u 96-18-4 u 10B-86-1 u 95-49-B 0.65 106-43-4 u 541-73-1 0.67 ET 106-46-7 u 95-50-1 u 96-12-8 u 120-82-1 u 87-68-3 u 87-61-6 u 1634-04-4 u 71-43-2 u 108-88-3 u 100-41-4 u 108-38-3 u 95-47-6 u 100-42-5 u 98-82-8 u 103-65-1 u 108-67-8 u 98-06-6 u 95-63-6 u 1 35-98-8 u ~9-87-6 u I 04-51-8 u 91-20-3 - 1,2,3-Trichloropropane B101nobenzene 2-Chlorotoluene 4-Chloroto!uene 1,3-Dichlorobenzene 1,4-0ichlorobenzene 1 ,2-0ichlorobeniene 1, 2-0ibromo-3-Chloropropane 1,2,4-Trichlorobenzene Hexachlorobutadiene 1, 2, 3-T rich1orobenzene Methyl-tert-butyl ether Benzene Toluene Ethyl benzene m,p-Xylenes o-Xylene Styrene lsopropylbenz:ene n-Propylbenz:ene 1, 3, 5-Trimethylbenzene ter t-Butylbenz:ene 1, 2,4-T rirnethylbenz:enc sec-Butylbenz:ene p-i sop, o pyl tolu en.:! n-Butylbenzene Naphthalene Other purgeables detected {up to 10 highest pen ks) - -LAB NO. 5G1746 SUPERVISOR DATE ENTERED BY CHECKED BY 0.25 1 0.25 0.25 0.25 0.25 0.25 1 0 25 0.25 0.75 5 2 0.74 Deiected uy/L NO VOLATILE ORGANIC COMPOUNDS QUANT IT ATEO BY GC/PID. lJ u lJ u lJ lJ u lJ lJ u u u lJ u u u lJ u u u u u u lJ u u I I I I I I I I I I I I I I I I I I 'I State of North Carolina Department of Environment, Health and Natural Resources Mooresville Regional Office James B. Hunt, Jr., Governor Jonathan B. Howes. Secretary Vivian H. Burke. Regional Manager _&-•!TA -___ •fJl~ n n rt'------• DEHNR DIVISION OF ENVIRONMENTAL MANAGEMENT May 2, 1994 Florence Russell Route 14, Box 356 Statesville, North Carolina 28&77 Dear Ms. Russell: RE: Well Water Sample Results Morgan Well Iredell County, N.C. On March 15, 1994 staff from the Mooresville Regional Office of the North Carolina Division of Environmental Management sampled your well at Route 14, Box 356, Statesville. The samples were analyzed for volatile organic compounds, nitrate and mercury. Volatile organic compounds include a wide range of manrnade compounds including, but not limited to, gasoline components and chlorinated solvents used as degreasers. Lab=atory results from these samples indicate at the time of sampling that volatile organic compounds, mercury and nitrate were present in your water supply. A copy of the laboratory results is enclosed for your review. These results are: Compound Concentration* EPA Drinking Water Standards* 1,1-Dichloroethane 1,4-Dichlorobenzene Nitrate/Nitrite Mercury .59 .53 8. 2** 2.85 +North Carolina Groundwater Standard 100+ 75 1 0 / 1 ** 2 *Concentration in micrograms per liter (ug/1), which is also rarts per billion (ppb}. *concentration in milligrams per liter (mg/1), which is also parts per million (ppm). Mercury exceeds the drinking water standards. I will forward a copy of the laboratory results to the State Toxicologist, and request a written evaluation concerning health risks for human consumption. I will forward those comments to you upon receipt. 919 North Main Street. Mooresville. North Carolina 28115 Telephone 704-663-1699 FAX 704-663-6040 An Equal OpporlunHy Affirmative Action Employer 50% recycled/ l 0% posl-cor.sum·er paper CIY? J) I I. I --- 1 I I_ I I I I I I I 1· I I I I I ·Ms. Florence Russell May 2, 1994 Page Two Should you have questions in the meantime, please call me at ( 704) 663-1 699, ext. 235. Enclosure: Lab Results Sincerely, Chris DeRoller Hydrogeologist cc: Iredell County Health Department Mary Sigmon -AAA Enterprises CMD/sc I I I . I I I I I I I I State of North Carolina Department of Environment, Health and Natural Resources Mooresville Regional Office James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary Linda Diane Long, Regional Manager Florence Russell Route 14, Box 356 DIVISION OF ENVIRONMENTAL MANAGEMENT May 2, 1995 Statesville, North Carolina 28677 RE: Health Risk Assessment Florence Russell Well Iredell County, N.C. Dear Mrs. Russell: Please find attached a copy of the Health Risk Assessment performed by Dr. Ken Rudo on·your well located at Route 14, Box 356, Statesville in Iredell County. If you contact Dr. ext. 243. KDW/sc Attachment should have any questions 1 please do not hesitate to Rudo at (919) 733-3410 or me at (704) 663-1699, s~~~ l~O/L Karea Walker ~ Hydrogeologist cc: Iredell County HeaLth Department 919 North Main Street. Mooresville. North Carolina 28115 Telephone 70A·663· 1699 FAX 70A·663·6040 An Equal Opporrunity Affirmative Action Employer 50% recycled/ la% post•consumer paper ! I_, 1. I I I I I I I I I I I I I Nn"t"th carnlina N.C. DEPT. OF ENVIRONMENT, HF..' -·. Department of Environment, Health, , Natural Resource'!!· REsr• Divi&ion of Epidemiology Environmental Epidemiology Section APR 26 bJ Drinkin; 'Nater Health lU.ak !valuatiot1 , ,,,,,nr--i""'l'l I"'-'. DJli1'J C " .,.,1 ''" ,. "" General J;~ou~,siitLbbW,~ om,_, L11BORATORY NUMBE.R __ ...:.5:..~;..(-_J6_6 __ _ ( ) Based on these analytical results, this water should be considered safe for normal usage. (l:emical an11lysis did not sh0\11 any contamination. 'Nater should be reau;,led if odor or taste persists. ( ) The water should not be used for drinking or cooking purposes, avoid prolonged bathing/showering. ( ) Based on these analytical results, this water is highly contaminated and should not be used for drinking, cooking or bat.hing/1howering. ( ) The laboratory re&ults are not conclusive, please reslll!lPle: For further information, contact Dr. Xen Rudo or Dr. Luanna 'Nillimns, Environmental Epidemiology Section, (919) 733-3410, DEl!NR 3B91 (5/92) Environment11l Epidl!Il'~ology Section (Review 5/95) ----- - -----·----- - I I I Counly __ :r:_r~e_c~lcce._l_l -----------'- Quad No Llo1 " -'6 Lat. .35° '/;)' 58 ,, Serial No. ______ _ Long. Bo· Sil' I 8 '1 Report To: ARO, FRO,@RRO, WaRO, WiRO, [Jy' SAMPLE PRIORITY ~ROUTINE □EMERGENCY ~CHAIN OF CUSTODY WSRO, Kinston FO, Fed: Trust, Central Off., Other: ________ _ Shipped by: Bus, ~Hand Del., Other_· __________ _ North Carol Ina Oepartmenl ol Environment, Health, and Natural Resources DIVISION OF ENVIRONMENTAL MANAGEMENT· GROUNDWATER SECTION 0 Other: -----c,------t=r-+-~----- Data Entry By:_.,,<2t/--½--,----C••iib %/£; Date Reported: ______________ _ Collector(s): kw cu 1'-''-• Date ~ -L<> • <\ 'S FIELD ANALYSES Purpose: Time \ ':l ~ ~ V p,._,,, Baseline, Complaint, Cornpliance1 LUST, Pesticide Study, Federal Trust, Other: Poi\ 1,,.;Koo t1n 0 \\t.ci~ crcl• on.) Owner ~k,(<2r><.f '?.l.G'.>;';,c,\\ (\3;1,-,c,C>du.. Morgv::, c,vJ,.g_,') 6wT ...... '3~l.L·c;·,,j"OnS pH400 \.o ,0 Spec. Cond . ., C::::::: at 25° C Location or site AoJ;..t,,.. IL\ 6m: 35<. , 5-\o;l es pi J le Ne. z •<a'] '7 Temp.10 ::;;::-----0c Odor _l"\.D~~NL~~---Description al sampling point \•,,h:x)~ n S,n k SpitJ:r\:: Appearance c,),g_Q£ Sampling Method ~F~lA~"'~f.>~-c-----==-==cr--------Sample lnterval_=l.,Ul-.l~~<JL~_•ufh.~-- < _ J. r--IP,.,.-rc:i,b:.•,.•1<:I .... c::-• Field Analysis By: ):',,u)o,..L\c.o,,,. Remarks ..=,<..ehQ\eu o...,..t • C p1,1,t:1,0\n') -"""' oS -"T" '\ tpuifl,ing llmto. •• l.«ip_ 9IC I LABORATORY ANALYSES BOD 310 ma/I Diss. Solids 70300 mntl Aa -Silver 46566 ua/1 Organochlorine Pesticides COD High 340 mg/1 Flouride 951 mnn Al -Aluminum 46557 uQ/1 Organophosphmus Peslicides COD Low 335 mn!I u .. ,dne ..... • T nlal 9nn 1n!il As• Arsenic 46551 untl Nitrogen Pesticides Coliform: MF Fecal 31616 1100ml Hardness (non-carb) 902 m~I Ba • Barium 46558 uall Colilorm: MF Tolal 31504 /100ml Eh~a2I~ J~ZJQ ~g!] Ca • Calcium 46552 mn!I Acid Herbicides TOC 680 ma/I SQ~~ific CQnd, 25 !.!Mh2~s;;rn~ Cd -Cadmium 46559 untl T urbidily 76 NTU Sullale 945 mnil Cr • Chromium 46560 unn Semivolatile Oroanics Residue., Suspended 530 mg/1 Sullide 745 mqt1 Cu -Coooer 46562 uQ/1 Fe -hon 46563 uQ/1 >< Hq -Mercury 71900 S-? uo/1 >< Volalile Otganics (VOA bottle) pH 403 unils K -Potassium 46555 mg/I Alkalinily lo pH 4.5 410 rngll Mg -Magnesium 46554 mg,'1 TPH -Gasoline Range Alkalinily lo pH 8.3 415 mg/1 Mn -Manqanese 46565 uQII TPH · BTEX Gasoline Range Carbonate HS ' mg/I NH. as N 610 O, Oq mQII Na • Sodium 46556 mail -~ ,.,,,,P'f. 0¥ Bicarbonate 4-40 mn!I Jtifj as~ 625 mg/I !:Ji · tJi~h~I ~g!] ·,..:,.,,..,1.E,NT, ru:..,,;..:--_-7c.• Carbon dioxide 40!1 moll X NO, + ~O, as N 630 9,':l mg/I Pb . Lead 46564 unil ~•-· NP.,.'f\j\ll\L ., ..... - Chloride 940 moil P: Tolal as P 665 mG'I Se • Selenium uail \ I .aar Chromium: Hex 1032 uall Zn• Zinc 46567 ug,'I I/ !\\ll\ 1 ~ ,,,. Color: True eo Pl-Co V Cyanide 720 mg/1 ., ,.,,,.,nv,~rn'"L i:J,i\1\'.l)lt~\- "" '"' ... irnio, .. , ...... Lab Comments: -----------------------------------------------~f.·~o._,._.,_it_ll_l ______ _ GW-54 REV For Dissolved Analysis -submit lilte,ed sample and write "DIS" in b -·· - -- REPORTED BY CHECKED BY REVIEWED BY SAMPLE TYPE: 75.35.4 75-09-2 156-60-5 75034.3 590-20-7 156-59-4 67-66-3 74-97-5 71-55-6 563-58-6 56-23-5 107-06-2 79-01-6 78-87-5 75-27-4 74-95-3 1DD61-O1-5 1 OD61-O2-6 79-00-5 127-18-4 142-28-9 124-48-1 106-93-4 108-90-7 630-20-6 75-25-2 79-34-5 TOL- T- E- U- N- 0- M- COMW ·s: ------; WATER 1, 1-Dichloroothene 0.75 Methylene Chloride 10 trans-1,2-Dichloroethene 0.75 1, 1-Dichloroethane 0.25 2,2-0ichloropropane 0.25 cis-1,2-0ichloroetheno 0.25 Chloroform 0.25 Bromochloromethane 0.75 1, 1, 1-Trichloroethane 0.25 1, 1-Dichloropropene 0.25 Carbon Tetrachloride 0.75 1, 2-Dichloroethane 0.25 Trichloroethane 0.25 1,2-Dichloropropane 0.25 Bromodichloromethane 0.25 Dibromomethane 1 cis-1,3-Dichloropropene 0.25 trans-1, 3-Dichloropropene 0.25 1, 1,2-Trichloroethane 0.25 T etr achloroethone 0.25 1, 3•Dichforopropano 0.25 Dibro1nocl1lorometl1ano 0.75 1,2-Dibrornoethano 1 Chlorobenzene 0.25 1, 1, 1, 2-T etrachloroetllane 0.25 Bromoforrn 0.5 1, 1,2,2-Totrachloroothane 0.75 Target Quantitation Limit-Subject to Chango due to instrument sensitivity Tentatively Identified, not confirmed Estimated Value Samples analyzed for this compound but not detected Sample not analyzed for this compound Detected below quantitation limit GC/MS Analysis performed EHNR/DEM LABORATORY VOLATILE ANALYTICAL REPORT ANALYSIS RES UL TS u 96-18-4 1,2, 3-T,ichloropropane u 108-86-1 Brornobenzene u 95-49-8 2-Chlorotoluene 0.72 106-43-4 4-Chlorotoluene u 541-73-1 1, 3-Dichlorobenzene 0.43 106-46-7 1 ,4-Dichlorobenzone u 95-50-1 1,2-Dichlorobenzene u 96-12-8 1,2-Dib,omo-3-Ctiloropropane u 120-82-1 1,2,4-Trichlorobenzene u 87-68-3 Hex achier obutadiene u 87-61-6 1 ,2, 3-Trichlorobenzene u 1634-04-4 Methyl-tort-butyl ether 0.27 71-43-2 Benzene u 108-88-3 Toluene u 100-41-4 Ethyl benzene u 108-38-3 m,p-Xylenes u 95-47-6 o-Xylene u 100-42-5 Styrene u 98-82-8 lsoµropylbenzone u 103-65-1 n-Propylbenzeno u 108-67-8 1, 3, 6-T rimethylbenzono u 98-06-6 tert-Butylbonzono u 95-63-6 1,2,4-Trimothylbenzono u 1 35-98-8 sec-Butylbenzene u 99-87-6 p-isopropyltolue no u 104-51-8 n-Butylbenzone u 91-20-3 Naphthalene Other purgeables detected (up to 10 highest peaks) FOUR UNIDENTIFIED PEAKS DETECTED BY GC/ELCD, ONE UNlDENTIFIED PEAK DETECTED BY GC/PID. LAB NO. 5G306 SUPERVISOR DATE ENTERED BY CHECKED BY 0.26 1 0.25 0.25 0.25 0.25 0.25 1 0.25 0.25 0.75 5 1 2 0.87 D D Detected- ug/L u u u u u u u u u u u u u u u u u u u u u u u u I I J II I Ill I II I I I I I I I I ,-- 1 I State of North Carolina Department of Environment, _Health and Natural Resources Mooresville Regional Office James B. Hunt. Jr .. Governor Jonathan B. Howes. Secretary DIVISION OF ENVIRONMENTAL MANAGEMENT February 7, 1996 Florence Russell Route 14, Box 356 Statesville, North Carolina 28677 Dear Ms. Russell: RE: Well Water Sample Results Morgan/Russell Well Stanly County, N.C. -I.-,4-<-U- On October 10, 1995, staff from the Mooresville Regional Office of the North Carolina Division of Environmental Management sampled your well at Route 14, Box 356, Statesville in Iredell County. The samples were analyzed for volatile organic compounds, nitrate and mercury. Volatile organic compounds include a wide range of manmade compounds including, but not limited to, gasoline components and chlorinated solvents used as degreasers. Laboratory results from these samples indicate at the time of sampling that volatile organic compounds were present in your water supply. A copy of the laboratory results is enclosed for your review. These results are: 1,1-dichloroethane cis-1,2- dichloroethene 1,4-dichlorobenzene nitrate/nitrite mercury 919 North Main Street. Mooresville. North Carolina 28115 Voice 704-663-1699 0.65 0.67 0.74 8.6 5.4 700+ 70 75 10/1 2 FAX 704-663-6040 Ari Equal Opportunity/ Affirmative Action Employer 50% recycled/10% post-consumer paper I I I I I I I I I I I I I 1- 1 I Ms. Russell February 7, 1996 Page Two *Concentration in micrograms per liter (ug/1), which is also parts per billion (ppb). +North Carolina Groundwater standard **Concentration in milligrams per liter(mg/1), which is also parts per million (ppm). Based on these results, you should continue to use bottle water. Should you have questions, please call me at (704) 663- 1699, ext. 243. Enclosure: Lab Results Sincerely, Karen Connell Hydrogeologist cc: Stanly County Health Department KWC GROUNDWATER FIELD/LAB FORM •',U"Toru, North Carolina "L; ~ l)~porlment of Environment, Health, end Nelurel Resources · DIVISION bF ENVIRONMENTAL MANAGEMENT, GROUNDWATER SECTION County ,J.., ~ocltU Quad No U,'7n-6 Lat. ·sso1J·J" 5£11"1 ,. -~•r rw ,_ I I ML' I "'. --._, _T;kab Number ----.., -::, ~~'-1~\Q~~~~~-- SAM PLE PRIORITY ,,,.,.,-:,. •o·•· -· 'Date Recei\!ed \D\ II \C\C:::, Time /0 ::J:::) Serial No. ______ _ P-o~ ~a/ Long. ~ ._Jr, I a,, (_) [JROU~~Hlllg:~~~~~~~; .; -.. • ;_ , -,-.. _, ,-··-~:~~:by: 4P 1 ~Ous~ Hand Del, Report To: ARO, FR~~ RRO, WaRO, WiRO, lXJ ,Pala Entry By: 7/-c'..----Ck: _©-""'-5_L., ___ _ WSRO, Kinston FO, Fed. Trust, Central Off., Other:_________ :;,:i, 'O~te Reported: / J' 7·:q,,., 7& Shipped by: Bus.~~~'Hand Del., Other·______________ Purposo: -.--• c: V-,' J,,cll il'/ J:1 Collector(s)://(' en a i'./1 Date 10-IO .q ~ Time /1: 3-5 A,......., Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trusl, Othor· \1.!.tLLL11 i:n 11,•n.i It., c,c• _ i· _ 1 J 1cucle ona) ,1 EIELD ANALYSES Owner H0,u'-'u_, "'-'-'-""u.'--'---' pH, 00 (,,. u Spec. Cond. 94 t'-/{!u;,J,n at~5° C Location or site 6D1Ltc d , l.fo.'< -3-:S 0 Sh.tw •-'' /I, 1 J--1 ( 2. 'i! l· · 1 -, Temp.10 11,,,'.5 °c Odor 11011 Description ol sampling point .li1L·.,'-'f-""h~•~,>~,.,_f"'J,~1.u"'·-"t_l(~~k~,~'~"~·(~---------~-------- Appearance r Sampling Method Cic.<-1p Sample lnterval,....:cf,'-',-'-''-'11'-'-,_,_1' ____ _ {' < ... , _ r {Pump,b.i1le1.•1c) ) ( . ., Jr ~ - Field Analysis By: k l'O n e I I Remarks ~/2-~',-'-~-f'LLJc,__"'f-,._, x-bcc-:,.; ~•=• l,:';;;·r=-=-=cc;:J--.'''--'.,.-,--'-'--'' •.LJ .,_, ______________ _ l} -,---(pumping 11m•. 11r 1•mp. etc) LABORATORY ANALYSES, OOD. 310 mn/1 Diss. Soljds 70300 mg/I An -Silver 46566 uQ/1 Oraanochlorine Pesticides -- COD High 340 mg/I Flouride 951 mQ/1 Al -Aluminum 46557 uq/1 Organophosphorus Pesticides COD Low 335 mg/I Hardness: Total 900 rrJgiL As -Arsenic 46551 ua/1 Nitroqen Pesticides -- Coliform: MF Fecal 31616 /100ml Hardness lnon-carb\ 902 mn/1 Ba• Barium 46558 ua~ Coliform: MF Total 31504 1100ml E!~D.Q~~130 --ug/1_ Ca -Calcium 46552 mn,I Add Herbicides TOG 680 mg/I -.Sned!ic Cond. 95 uMhQ~£.rn~-Cd -Cadmium 46559 ugt! -- Turbidi1y 76 NTU Sulfate 945 mg/!_ Cr• Chromium 46560 ug!I_ Semivolatila Organics ---- Residue., Suspended 530 mryl Sulfide 745 n~g{!_ Cu -Cooper 4GSG2 ug!I_ ---- l~x Fe -Iron 46563 u9'1_ Ha -Mercur}'. 71900 ,; l/ ugll >< Vola1ilo Organics (VOA bollle) pH 403 unit~ K -Polassium 46555 mg/I Alkalinily lo pH 4.5 410 mg/I _!,,lg -Magnosium 46554 mg/I TPH -Gasolino Range l\lkalinily 10 pH 8.3 415 mgll Mn -Manganese 4G5G5 ugll TPH · OTEX Gasoline Range --Carbonate 445 mgll NH as N 610 o.o ~ moll Na -Sodium 46556 mq/1 Bicarbonate 440 mn/1 .IKti.as_N_62' \l'L Ni· Nickel ugl)_ ; ---- Carbon dioxide 405 mn/1 ~ _HQ + NO~s N 630 }';' (,, 11!9'L Pb -Lead 46564 ug/1 I / Chlorido 940 mg~ P: Total as P 665 mg/I_ Se -Selenium ugll V Chromium: Hex 1032 u[JII Zn -Zinc 46567 ug/1 Color: True oo P1-Co --Cyanide 720 mgll I.ab Comments:-------------------------------------------'----------------- Gw r.1 f'!I=\' • For.Dissolved Anc1tysis • submit filt~red s~mnlp and writfl "DIS" in I -\• -i--l --------l ------ ----r: EHNR/DEM LABORATORY LAB NO. 5G1746 ~ VOLATILE ANALYTICAL REPORT REPORTED BY SUPERVISOR ,-,:;,<'.' / ¥ CHECKED BY DATE 'J·I .1_S- REVIEWED BY ENTERED BY CHECKED BY /-,<_/.9/91 --- SAMPLE TYPE: WATER ANALYSIS AESUL TS / 7 75-35-4 1, 1-Dichloroethene 0.75 u 96-18-4 1,2,3-Trichloropropane 0.25 u 75-09-2 Methylene Chloride 10 u 108-86-1 Brornobenzene u 156-60-5 trans-1, 2-DichlorOethene 0. 75 u 95-49-8 2-Chlorotoluene 0.25 u 75-34-3 1, 1-Dichloroethane 0.25 0.65 1 06-43-4 4-Chlorotoluene 0.25 u 590-20-7 2, 2-Dichloropropane 0.25 u 541-73-1 1, 3-Dichlorobenzene 0.25 u 156-59-4 cis-1,2-Dichloroethene 0.25 0.67 E T 106-46· 7 1 ,4-Dichlorobenzene 0.25 0.74 67-66-3 Chloroform 0.25 u 95-50-1 1,2-0ichlorobenzene 0.25 u 74-97-5 Bromochloro rnetha ne 0.75 u 96-12-B 1, 2-Dibromo-3-Chloropropane \J 71-55-6 1, 1, 1-Trichloroethane 0.25 u 120-B2-1 1, 2,4-T richlorobenzene 0.25 u 563-58-6 1, 1-Dichloropropene 0.25 u 87-68-3 H exachlorobu tadiene 0.25 u 56-23-5 Carbon Totrachloride 0.75 u 87-61-6 1,2, 3-Trichlorohenzene 0.75 u 1 07-06-2 1,2-Dichloroethane 0.25 u 1634-04-4 Methyl-tert-butyl ether 5 u 79-01-6 Trichloroethane 0.25 u 71-43-2 Benzene u 78-87-5 1,2-Dichloropropane 0.25 u 1 OB-88-3 Toluene u 75-27-4 Bromodichloromethane 0.25 u 100-41-4 Ethyl benzene 1 u 74-95-3 Dibromomethane 1 u 108-38-3 m,p-Xytenes 2 u 10061-01-5 cis-1,3-Dichloropropene 0.25 u 95-4 7-6 a-Xylene u 10061-02-6 trans-1,3-Dichloropropene 0.25 u 100-42-5 Styrene u 79-00-5 1, 1,2-Trichloroethane 0.25 u 98-82·8 lsopropylbenzene u 127-18-4 Tetrachloroethene 0.25 u 103-65-1 n-Propylbenzene u 142-28-9 1,3-Dichloropropane 0.25 u 108-67-8 1,3,5-Trimethylbenzene u 124-48-1 Dihromochloromethane 0.75 u 98-06-6 tert-Butytbenzene u 106-93-4 1,2-Dibromoethane u 95-63-6 1,2,4-Trimethylbenzene u 108-90-7 Chlorobenzene 0.25 u 135-98-8 sec-Butylbenzene u 630-20-6 1, 1, 1,2-Tetrachloroethane 0.25 u 99-87-6 p-isopro ryltolueno u 75-25-2 Bromoform 0.5 u 104-51-8 n-Butylbenzene u 79-34-5 1, 1 ,2, 2-Tetrachloroethane 0.75 u 91-20-3 Naphthaterie u TOL-Target Ouantitation Limit-Subject to Other purgeahles detected Detected change due to instrument sensitivity {up to 10 highest pen ks) ug/L T-Tentatively Identified, not confirmed E-Estimated Value NO VOLATILE ORGANIC COMPOUNDS OUANTITATED BY U-Samples analyzed for this compound but not detected GC/PID. N-Sample not analyzed for this compound D-Detected below quantitation limit M-GC/MS Analysis performed COMMENTS: ,---r .. I ---- - - - - --- -----.. -- I I I I I I I I I I I I I I I I I I I State of North Carolina Department of Environment, Health and Natural Resources Mooresville Regional Office James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary Rachel Brown 183 Lauren Drive --♦ IMdAF¥1 DEHNR DIVISION OF WATER QUALITY January 10, 1997 Statesville, North Carolina 28677 Dear Ms. Brown: RE: Health Risk Evaluation Brown Well Iredell County I have enclosed the health risk evaluation for the water sample taken from your well on October 7, 1996. If you have any ~uestions, please call me at (704) 663-1699, ext. 234. Enclosures cc: James Beam \prd\brown. hrl 919 North Main Street. Mooresville. North Carolina 28 115 Voice 70'1-663-1699 Sincerely, ~-~=> "'-~ Paul R. Dahlen, P.G. Hydrogeologist FAX 70'1-663-60'10 p:i!tj LI .j #JI An Equal Opportunity/ Affirmative Action Employer 50'% recycled/10%, post-consumer paper I ., ' I I I I I I I I I I I I I I I I I I NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEAL TH. AND NATURAL RESOURCES DIVISION OF EPIDEMIOLOGY OCCUPATIONAL AND ENVIRONMENTAL EPIDEMIOLOGY SECTION DRINKING WATER HEALTH RISK EVALUATION GENERAL DATE /1"/li/7 b COUNTY __ _;::_J:~~=-~·---LABORATORY# __ 6_?_z_z_3_} __ ( ) ( ) ( ) Based on these analytical results. this water should be considered safe for normal usage. Chemical analysis did not show any contamination. Water should be resampled if odor or taste persists. The water should not be used for drinking or cooking purposes: avoid prolonged bathing.lsho\1,-•ering. Based on these anal;1ical results. this water is highly contaminated and should not be used for drinking. cooking . or bathinglshowering. The laboratory results are not conclusi\'e. please resample. PLEASE INDICATE 01\ LAB SHEET THAT IT IS A RESA~IPLE A'\D PRO\'IDE PRE\'IOL:S SAMPLE NUi\lBER(S). CO~IMENTS: For further information. contact Dr. Ken Rudo. Occupational and Environmental Epidemiology Section, (919) 715-6430. DEH:-iR 3891 /51961 Occupational and Environmental Epidemiology Section (Re\'iew 5/991 l"'otn10 11lU·Crntt(S) ·::_t, l E· ·~·•1F.: -• PPOSE· '-' \llOHATOlff ANALYSIS ,u .=, non110 C'OD!lipllo CODl.o"·JJl Coliforno; MffculJl61ti C,c,1,fom.; MFToul ]!50. roe r,-1,irity ~,\idu.e .• 5'i'P(Mod HO . Tot.i.lSu~,ot.d, - '" - 1>,Lu.l11u1,mc,114, -A1\,.;.liM)'tDpHl.l" ·- (IIObc,,,tak D>Ca"btw>Me c .t-o.r. dinxid, O,lixi<M: .. ·- t.mo■1i .. r-· lln IOU Cc,loo-: Tn~ SO --c~ ilJOOC no IMM£NHi: liiiiiil iiiiil ·-,..,_ rm~•L ..,~ .... ·,. -' /JfJio:nJ ·. /llnnJ . ...,, Nlll ,,,,.'L ll>S'L. , ... ... , .. .., ..... 1. .,.,,_ ••11"-.,~,,. ... i;."l. ..,,_ -C:~ .· ...,,_ - J~11pn,>o, of ='"f>li.g point Sal'lflin~ Mclltood Rcm..J\1: ------· Om. Solids IQ\.IIO --t'luoridl: <>51 ~it-dnes1: tobl ~Xl ti1a~ (~) 90: -r,.uno ---if-= coro.. 95 Sc.!bff !..Jl(,&: US MJ\AS O■li,ndO,..,_ Sific-3 Ooran WO OH H 610 lt:Nutl61'j X N01 +NO.l 1s i, 610 P'. 1c,o1.., Pt.6~ "" . - - l>l\'[."iJtJN 01,· •:NVIRONMENTAL f'\1AN1\GEMl:Nf ~Ml't~f"..!.!<J.R_I!\ ~RIMITINF. ~ Ol,\lr,l()fl:t/S-IOIIY E:J SAMJ1 l:: 1 YrE ITT r:MHI.GEl!CY □ ·1 :1: :; .. I . I qo i:rs: '-··1 ,~; •:-_• :.-· · ·,_=•r -1 t 1: ... 1 :n 1, ;:,, i'.1:',--l'i_•:~·\!, 1-:i•.:·::_Ylll•I:_~;~:'.; WlV _______________ ..l/il· .. , .;u''Ul...ill:U,r.,;u,a1,1 l?AlAGUHI ----------------11D;;r.l,;i~I[ Rccmm lllH,E 11,&11. !\~•Sit.,:, .C616'i ufYL m&IL ._I J\mnl••un .«,!iH ""l mo{l A,-.An.e:nic .C65j I ,.,n. moll &-B.-ium-t.655! ,.,,. UfJ\. Ca-Calci ... .t6.SS2 ..,,_ u"1hoslo"2 r:d--C.ati<,m%5!i9 ..,_ 11'@.ll. 0-{...........,-46-~ ...... ....,._ C■-l"OQV'Cl" IOU ..,_ ,..,,. r.-.111x1 JO-U -,,t. --' 111--Mrrn•r 11<11'."0 5.1 ..,,_ ,nyl. 1-r<"lni.iuai 4M:'I! --I.le.-M.-,,CW,,.. 911 ■nwt: -.., ... ~1zy,;5 .. ""' 0.01 ••!l,>1.. tla-~iu ... 92? ..,, ~&IL N>-NOCk,rl ""' 7.3 ""'l n.-Ln■:t'-4~ ""'· msl\-St--St:Lciiu-. ..... , ... ,l b 7..mc4£i~, ,,., -. ,. • • - - - ---- - - IJ.N,.d><T mrn 11:w:R~ ..... I : , .... l"ilf>C """"'il'Cd : 9".lO,\M R~th~I B1 "" . Rdu-ffl By : "' l>.m ,q,u,1~: nu.~ O,,~IOOa.: l't~r,. O.p;-t~o.., fe.li..:io.b. tfitntg,mP-~ . . Acid I te,-hici&:,; - L~ .. .-i1rt: rPH-Dic:m R•lf\C - Vota,iil-t <J■s,ur,ia!Vt!A ~le) IPH-Gawlr.c R.~c TPII-BfEX C--.oli■>t R:a-'1:!'t . ---- IL-' REPORIEL> 8Y CHECrJ:D flY REVIEV'tEU BY ::.AMPLE. rYf•E: 75.;is-4 75-09·2 15G-GO·S 75-J4-3 590,?0-7 156·59--4 67.fifj-J '/4-97-5 71-55-0 563-Ss.-.3 56-23-5 107-06-2 79-01-6 7B-IH-5 /5,-27 ..... 74--95.-J 10061--01-5 10061-02~ 79-00-5 127-18---4 1-4.2-28--9 12-4.--48--1 106-93-4 _ 108-90-:7 6J0-20--8 75--25--2 79-3--4.-5 IOt .. · T- E- U- N- l,l-Di~he11e Me<.11,-ie.v.; Chl:lfide lmns• 1,2-0ictLoel!.ene 1, 1-0iclilJrceth.tne 2.~-0ichbrqKO{lilne cis-1,2-0ichlot0t.!!l,e11e Chkxofom, Bromcchloromcthanc 1.1.1-TrichlOf"oeltlane 1.1-0ichbrCf)fopene _ Carbon letrarlllorkle 1,2-Dictll'.:lroetlwne Trichloroetl~: . 1.2-DichbropropaM ~•on1odich!01ornelhaoo Dib.omome(hane cis-1.3--Dictlloropr~ llans--1.3-0ichloropf opene 1, 1,2-Tri:MoroMhane 1 ek ac:1110.-oethi~ne 1,3--0ich~rJe Dibf01noch!ororneU1.ane 1,2-o.t.iromoeth.Jnc. Ctk:N"oberl.l.efle. 1, 1, 1.2-Tetrachloroclhane OrcnlOlonn I, 1,2.2-lctrachk:mdhane Target_CJt1.arJli!l;Jlion Um.ii-SL~~t I~ cha~ rt-.ie lo i~tru_rnent s.ensilivity. renla.livdy l~•tifiad. l't04 conf1med fatimaled Value O.i'5 10 D. 75 0 25 0.25 U.2.'> 0.25 0. ,s 0 25 0.2!> 0.75 0.2!°> 0.25 0.25 0.2& ., 075 0.25 0.25 0.25 ·. 0.25 0.7~ 1 - -0.25- 0.25 05 0.75- S.lmJJles analyzed Jor this compound bul no( ~elecled Sample nol aml'(Zed fOf !his cou1pound D--. Detected bek;:Jow Q1JanMati:>r\li01it M-GCtMS Anafy!'is perfcrmed COMMENTS: EIUIIUUE:M LABORAfORY VOLAH .. E ,-_NA.LYTICAI. REPORT 0.63 0.61 E. 0 ANALYSIS RESllU S u 11 u 11 u u LI u " u u " " " u u u u u u u lJ u u 96-1&-4 I, 2,J..-1,K'.hloop,l,p:ane 106-M-I O,omobenz.ct~ 95~fl-8 2-i:llb"otOluena 106--43--4 4-Chbroioluene 5111-73-1 I , 3-Uic:-Nvrohenz: enr. 1%--ili-i I, 4-Oic:hklrobel12-erie 95-~1 1 , 2-Uic:hlo<~lt"fHle %-12-B 1,2-0ibumo-J-Chloroptopw IR 120-82-1 1,2.4-Tncttorobenzetie 87-68--3 l!~~ie 87-61--6 I ,2, 3-11\d'kwotienzerie 153-4-CM--4 Methy1-tett-bul:(1 eltlf!f 71--43--2 B,,,.,ene IOB--1'18--3 TOOJeno 100--41--4 EUryt beruer1~ 103-38--3 rn.p-X~lenes 96-41..fj o-Xylarl8 1oo-42--5 Styrene .... , .. lsqllnprlborue.NJ 1ro-6S-1 n-Prop,,t,,nzene 106-61--8 1 .. 3,5--Trlme-t1Y'ft,eiu:eoe 90-06-6 to1 r-llUly(bruuerie 95--63-6 1, 2,<4-Trimeltry#,en.zen,e 1'3!,.-98-8 · sec-UufytbeJUenO 9937-6 p-isq:,ropytlolteoe 10-4-51-8 n-Butylbenz.eoe !31-20-J Naplil\8Fe~ OlhE.'f PlD9flables deteded (up to 10 highe---t peaks) PNU U~~IDENTIFIEO PEAKS IJEI EC TEO rtY GCIPIO. , LA.B NO .. 662133. SUPEH\.1S0P. ~'1?L;k. · __ .. . . DIil E -:=!f¥2~ EfHFRL~l",~-.. llATF: -- 0.25 I 0.25 025 D.25 0.2"J □.25 1 0.25 fl,25 o. 1r, s 2 """'--0 25 0.63 2.0 mgll Ddecled "9'L " u u 1! u " u u u ll u u u u .U u u u ll u u u u u u N --~~~~-------------------------------------------- !!!!!!I , 1!!!11111 '== , liiiii liiii --- ----- ---- - nfPOR I ED BY C11FCl:::'EO OV fit:VIEW'!:0 BY - SAMPL( TYPE: 62· 53-:J IOH-!J5-2 111 -4•1--1 95-57-8 !;41-73-1 1013-46-7 100-!il-6 95-50-1 95-•'Hl-1 IOS-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 BB-"15-5 tOS-67-9 sr •. et.-0 111-91-1 120-83-2 ,~n-02-1 91-20-3 l(}{i-47-B 07-Gl:!·3 59-50-l !11-57-6 77-47-4 88-06-2 95-95-4 9\-58-:-7 ·aa-74~ I :JI-~ l-3 20El-96-8 --·- WA.TFR N..111.lNE Pl IEtJ01. B1S(2-crn.U1t0l::l ilYL! E ti ll:R 2-CHlOflOJ-'1 IFUOL 1.3-DICI llOAOBENZH~E l ,4-DIGI LOllOB!::rtzEN~ rlENZYI. AI.COIIOt 1,2-DICl II Oll0REN7 FNE 1..tdE IHYL Pt IUIOl OISl2~CHL0110l5(]f'ROPYU F.TIIEfl .4-MEJHYL PHENOL N-NITROS0-01-N-PHOPYLAMl~IE HEX Aci 1.t.On6ET11 At~ E NllROMNZENE ISOPfmAONE 2-NI TRO Pt-lENOL 2,4~04METl·l'll PflENOL · B[Uzo,r. ACID BISl2-CltLOOOf:TUOXY1 MEl"llMJE 2.4-0ICHLORO PHEUOL 1,2,4-fRtClll onoRE:U?.EN( N/\PIITIIAlENF. .;~_ 4-C'HLOAoANitiNE -_. Hl.:XACI II OROBUTADltNE , 4-CtUOIIO-'.lME.l!IYlf11ENOl 1-METliYl. NAPH'fllALENF.. HEXACfllOROf:YClOPENTAfllENE_ 2,4,li-\lllCfLOHO PHENOL 2,4.5-lRICHLOno PIIE~Ol 2-CHLORO NAPIIHIALEN£ 2:N!TROA.Nl.lt-lE DIMF.ri-lVL PlnHAlATE: ACENAPtlTHYLENE·-· - ---... -- EIITlRIOEM tARORJ\TORY SEMl-V0LA TILF. AMl YTICAL llHOII f ANALYStS R(.StA.f!: 10 1J 506-20·2 1(.l I) 99-09-2 10 V 93-32-9 10 u 51-~8-5 10 u 100 02-J 10 \J 132-64-9 70 u 11.,-U-2 IO u 84-66-2 "' lJ 7006-12-3 10 IJ 86-73-7 10 u 10001-6 lo u 534-52-1 10 u 8&-J0-6 1U u 101-55-3 10 u 118-74--1 10 u 87-86--5 10 u 85---01-B 511 u 120·12•7 lO 11 84-74-2 10 u 106-44 0 10 l) 12900-0 10 " 85-66-7 ,0 u· 91-94-1 10 V 56-55-3 2(1 u 218-01-9 lO " 117-81-7 '" 1) 117-04-0 10 l1 1()5-90·1 10 lJ 207•00-9 10 lJ 50-32-8 50 lJ -19"3-39-5 10 u 53-70•3 lO u 191-24-2 -__ !_ l!!!!l!!!I . . I!!!!!! m=I j =:;;a_i liiiii [ LAB NO. l:iiG223J SUr1;RV1$0R. i_. L., -=~ OAl E _(.tl ·Gi, ENTERED BY~ DAIE1JfB_I~ 2. £i.OINITflO IOUJENE 10 IJ J-NtrROAHll lt1E so V /1.C[N/\PI 11 HENE ,0 u 2.4-0INlfRO PHENOi. 50 V 4-rm no PHEUOt 50 u DlBENZOfUMN 10 V 2.4-0IN'I ntOlOLUENI:: 10 IJ DIETIIVL PtllHALATE 10 I) 4-Cf-lLOIIOPUENY\. PHFNYL ETHln 10 u n.oonEHE 10 u 4-NtTROANH.!NE 50 u 4.6-0INllll0-2-MElHYI. PHi:NOL 5:o " U-Nll110S00lf'IIENYLAM.1N€ 10 u 4-BROMOP1-IENYl F'11EMYL HK~ 10. . u HEXACHLOROBENZENE 10 u PEt-ITACIILORO PHENOL 50 u PHEUAtHIIRENE 10 V ANTURACEHF. 10 u Dl·N-mJTYL Pt-ffllALAT{; 10 IJ rLUOllANI IIENE · 10 u PYR'ENE. 10 V BUTTLBENZYL PHnlAJ.AT E 10 u 3.3'-CHCH.OAOBEffllDltE .. 20 u RENlO!AiANTtm ... cENE -,--Hi•'· lJ Cl!nYS(NE 10 lJ 81S(2-ETHYU-fEXYU PHH!ALA lE 10 u. OI-N-OCTYl Pl ITflALAl E 10 u RENlOtfllrLUC.IUANl tlEJ~E 10 ll D[NZO(KIA.LK>RANTI IF.Hf: 10 u BE:.NZOiAtP'YAE:NE .10 u INOENQ(l,2,3 CO)PY~El'iE 10 lJ D1BE:NZO[A.H}AHTHA~CEUE l(f • \J_ BENZOIG, ll,IJPERYLEHE 10 u --- COMMENIS; --·--------l!!!l!!!!I I!!!!!!!! st'MIVOU\TtlL OAOANICS Ra>OI\( -OiUI lAB l'AGE 2 ri+s.rt!Jtic 1! fire. .w UtJll)Ftfl IF!EU 22E LAB NO. ___ 6_G_2_2_3_3 TOl-l,'ll!]tl! Ouantitation Limit-Subiect t() ch:•n<JP. !Ille to instrument !':ensilivi1v T· T~itr,livuty Identified, tistiru:ttt!d cor1ctnlration E-'E!:.litnatf'd Val~Je U-Samples .inal\•zcd fCK this compound bu1 flOt d01ecled N-s ... n1fi,1 noL i111..lly1ed lor lhis cornpournl D-Oetocted bekiw quanlitation ltniit JI-floldill-{I tinic ai1ceeded l!!l!!!!I n 0 D R I I I I I I I I I I I I State of North Carolina Department of Environment, Health and Natural Resources Mooresville Regional Office James B. Hunt, Jr,, Governor Jonathan B. Howes, Secretary DIVISION OF WATER QUALITY May 28, 1997 Phyllis Frye 183 Lauren Drive Statesville, North Carolina 28677 Dear Ms, Frye: RE: Health Risk Evaluation Frye Well Iredell County I have enclosed the health risk evaluation for the water sample taken from your well on April 8, 1997. I will be resampling this well in July. If you have any questions, please call me at (704) 663-1699, ext. 234. Enclosures vCrd\£:ye.hrl 919 North Main Street, Mooresville, North Carolin□ 28115 Voice 70'1-663-1699 Sincerely, ~~ Paul R, Dahlen, P.G. Hydrogeologist FAX 70'1-663-60'10 Ar, Equal Opportunity/Affirmative Action Employer 50% recycled/]()% post-consumer paper u u· I I I I I I I I I· I I ( ) ( ) NORTH CAROLINA DEPARTME1'T OF ENVIRONMENT, HEALTH. AND NATURAL &Eso0'R'6E'{r.:: r'.:L. LTH DIVISION OF EPIDEMIOLOGY C, ;'.,\Tl; :C.\L ::.:o,ic :•,·:·.:s' OCCUPATIONAL AND ENVIRONMEN.TAL EPIDEMIOLOGY SECTION DRINKING WATER HEALTH RISK EVALUATION GENERAL MAY 20 1997 01v1::: : ~: ~::\·::.:::::;:::Et '.'.;t'.l~;c;,1rnT '' ,... >ell g;;,~rn CFfiCE COUNTY _L:,_h,..!.,;1~=---1_Jl_.:__· -LA BORA TORY# '/6-U/o// Based on these analytical results. this water should be considered safe for normal usage. Chemical analysis did not show any contamination. Water should be resampled if odor or taste persists. The water should not be used for drinking or cooking purposes: avoid prolonged bathing/showering. Based on these anal;tica\ results. this water is highly contaminated and should not be used for drinking. cooking . or bathing/showering. ( ) The laboratory results are not conclusive. pleJse-resample. PLEASE Ii','DICATE 0\ LAB SHEET THAT IT IS A RESAMPLE Ai'o'D PROVIDE PREVIOUS SA"PLE i','Li~IBER(S). COMME"'TS: :JI For further information. contact Dr. Ken Rudo. Occupational and Environmental Epidemiology Section, (919) 715-6430. DElf':R 389115/961 Occupational and Em·ironmental Epidemiology Section (Review 5/99) - C:OUNTY ')UAD NO: - lllEUELI, --------- l>l\'ISION OF WATEH <)I IA I.ITY SAMPLE PBIORJ fY ~ROUTINE 0Et.1ERGENCY ~El'ORTlO rimo Rcgimml Office :OLLECTOR(S) : ;D~,f\l~l~L~ENc,--------(D CllAINOl'llJS10DY ~ SAMl'LE TYPE □ JA l E: .CIB/97 IIME· 'IJRl'OSE: ,ABOHATOHY ANALYSIS uoo )10 n1g/L COU lligh 340 rug/L COD low JJS mg/I. Colifom, MF l'ccal )1616 /IOOrul Colifo1m· MF To1al J 15~ 1100ml IOC mg}l lurbitity NIU ltcsiJuc .. Suspended HO mg/I. fotal Suspended solids rug/L pll units Al~alini1y to pl! -l.S mg.IL Allaliuily 10 pl 18.J 11111/L Carbonalc mglL Bicaibonalc mglL Carbon dio,idc: mgll. 1·htn1i,lc m!!IL Chromium: l!c:x 1032 ,g/L Color: T,uc: BO '" Cy1midc 1'.!0 mg/L fl,\11\IENTS: Owucr· l.oca1io11 or fiilc: lluctiption of s:unplir,g poii,J Sampling 1'kthod: Remarks· Diss. Solids 10300 l'loo,idc: 951 I lardncss: total 900 I laiduc:ss: (non-carb) 902 l'hc:nols J27JO Specific Cond. 95 Sulb1c: Sulfide 7-IS MllAS Oil and li1case Silica Boron 1'01rnaldd,~·de NIIJasN610 IKNasN625 ., N02 ➔NOJasn610 I'. I 111al a, I' 6hS 1'04 l'!IYI.J.I.S nin: WEU. rui;/L A!!·Sihu 4oS66 rnWI. ,\1-Aluminuu, 46557 1111111. As-Arsenic 465S1 mg.IL lla-lla,ium 46558 ug/l. Ca-Calcium 465S2 ut.\hos/cm2 Cd-Cadium 46559 mglL (",-Chromium 4(,560 mg.IL Cu-Cu1•pcr IO 12 mg/L l'c-Iron 1045 "'!!''-' Ilg-1'1CICUI)' Jl')OQ -mg.IL K-Polassiu1n 46555 /Ilg· r-.lagncsium 927 lllf!'I. r-.1t1-1'lang:111csc 1055 0.01 mg,I. Na-Sodium '12'! mglL Ni-Nield S.2 "'f!IL l'h-1.c:id ![,fol rngll. Se·Sclcrnum 111gll. z., -Zrnc 465t,7 -l!!!!!!!I !!!!!I MAY 14 1997 DIVJ'i ::;· [:\~~~ilf~Ul ~AMAS[?.![, :_.•; ~-".iJ.i.E ifP.5".iM UT!'C[ Lnb N11111her 7<;0797 1Ja1e Reccisrd 4191'17 Time R.-cci,cd 9·J0 AM Rccci>ed lly ns Rdcnsed lly DS Pale 1cponeJ: 511 )fq1 ,., Org:mochlo1inc rcs1icidcs ,,,,, lltg:mophosphorus l'esiicides ugll. Niuogcn l'c:slicides ugl\. mglL Acid I le,bicidn uglL 111111. Scmi,ob11lcs ug.d. I rH-llicscl Range ug/L 2.5 ui;IL ' \'olati!c Ur!!il11ics (\'0,\ holllc) mgll. mg•L I Pl 1-G~~oline Range "!:!''-I I'll.II I EX (i3,olinc R3n!c(e ltl!_!•I. ug1I. u1_1II. uyll_ ugJl. 1G0797 APR -- -- - - - ---.. --111!1!!!1 !!!!!!!!!! . • ell == ' == . ' liiiiiiiiii ' \ J '! North Carolina GROUNDWATER FIELD/LAB FORM Deparlmenl of Environment, Health, and Nalural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION Serial No. _______ _ ~:..,,..,u ,•-w"· I? ''W Long. r:2d. Y L> 1 {. ') . . Report To: ARO, FRO, MBO, RRO, WaRO, WrRO, SAMe.LU'fl'!; a.water □soil D Other SAM E!&EfiLQ!l!D' :r:J.noullne D Emergency ----------- ~ Chain of Custody WSRO, Kinston FO, Fed. Trust, Central Off., Olher: _________ _ Shipped by: Bus,rr;;;;-;i~. Hand Del., Other_· ____________ _ 0 Lab Number Dale Received Rec'd by: Oilier: ___________________ _ Data Enlry By: ______ Ck: ______ _ Dale Reported: ______________ _ -,,_ ~ / . Prnposc: Colleclor(s): Ye, 11 I ei-... Date l.{ 2/51 Time ___fl · I:> Baseline, Complaint, Compliance, LUST, Pestici1Jo Sludy, Fedcrnl T,usl, Other: _. 7 _ . _ .Jcirdo 0110) , , FIELD ANALYSES I'-Owner 1-_l,!:JI/IJ. rr'Je W,"'.11 Ct ,,,,,,ocfJ R,,, 1,,1 1.•,c,,,o, ,,· 11) pt-1400 ,,_, (, v Spec. Cond.94 ~/'-.>"---'"-' _ at-25° C Location or site c~ · ;-.,,,.. . Temp 10 --~~-0 c Odor _______ Description ol sampling point --"k"'..l'>.c'c·l,<..o__\"-""U...------------------------ Appearance C ( ec.,--fee/ c.,-<.,,__,.J Sampling Method --------.. ",.-,-'--\--;-=--------Sample Interval ________ _ \ I ~,a,lnr. olc ) Field Analysts By: -~u~'"=~l~-t....~---------nemarks ---1.£.:,_i_,_, ,.._,,__:·0::,_..,,""----=---------------------------- LABORATORY ANALYSES "'""'"'""'"'· "' '""'" ""' BOD 310 1110/l Diss. Solids 70300 mq/1 An -Silver 46566 un/1 O,ganochlorine Pesticides COD High 340 mg/I Flouride 951 1119/I I Al -Aluminum 46557 un/1 O•ganoohosplmrus Pesticides -· -COD Low 335 mg!!_ Hardness: Total 900 mq/1 i As -Ai senic 46551 ug/1 Nit1oae11 Pesticides ColHorm: MF Fecal 31616 /1001111 Hardness /non-carbl 902 mall □a -Barium 46558 un/1 Acid Herbicides Colilorm: MF Tolal 31504 /1001111 Pt1enols 32730 ug/l Ca -Cc1lcium 46552 mall PCB's TOG 680 mg/1 .ll=i/kCond. 95 II MI l!lli.Qlf Cd -Cc1clmiurn 46559 ug/I -- Twbidily 76 NTU Sullale 945 mq/1 Cr -Chromium 46560 ur1/I Residue., Suspended 530 mg/I Sullicle 7 45 mall Cu -Copeer 46562 ugll --: Fe -Iron 46563 U!JII Sernivolalile Organics Oil and Grease mg/I z Hg -Mercwy 71900 ug/1 TPH -Diesel Range pll 403 unil~· K -Potassium 46555 mg/I Alkalinity to pit 4.5 410 mg/I Mq -Maqnesium 46554 mq/1 Alkalinity lo pH 8.3 415 mg/I Mn -Man!]anese 46565 uq/1 Carbonate 445 mg/I NH1 as N 610 mq/!_ Na -Sodium 46~50 mql.1 -;:;? Volatile Organics (VOA hotllo) -- Bicarbonale 440 moll IKN as N 625 mo.IL _tlLNil:ll O I "Oil TPH -Gasoline Ranne ~ -- Cmbon dioxide 405 mg/I NO. + NO~ as N 630 mg/I Pb -lead 46S64 uqll TPH -BTEX Gasollre Ranqe -- Chlo1ide 940 mg/I P: T olal as P 665 mq/1 Se -Seleniurn uq/I Cliromium: Hex 1032 ug/1 Zn -Zinc 46567 ug/I Color: True 80 cu Cyanide 720 mg/I Lab Comments:-------------------------------------------------------------- GW-54 REV. 7/' For Dissolved Analysis -submit filtered sample and w1ile "DIS" in blr ------· ---------l!!!!!!l!I I!!!!!!! IU:l'll/lll:1111( (:111'.Cl<l'.ll IIY l(FVl/'Wi-11 IIY 75-35-4 75-0!J.2 156-60-5 75-34-3 590-20-7 156-59-'1 67-66-3 7'1-91-5 71-55-6 563-56-G 56-7.3-5 107-06-2 79-01-6 78-87-5 75.27 .,1 74-95-3 10061-01-5 10061-02-6 79-00-5 127-18-4 142-28-9 124-48-1 106-93-4 108-90-7 630-20-6 75-25-2 79-34-5 TOL- 1- E- WAIi H 1, 1-Dichlorootheno Me111yle110 Ct11orido trnns-1, 2-Dic11loroolf10110 1, l-l)icl1loro1.1Umr10 2. 2-1 Jidllorop1 opnno cis-l,2-Uicl1lmoetl1e1ie Cl1loroform llror11ocl1loro1,ie!l1m1e 1, 1. 1-11ichloronlh11110 I. l-llicl1lorop1npe11e C;irbrm ·1n1rachloride 1.2-Dicl1!oroe!l1ane Trichloroe1hene 1.2-Dich!oropropane Brornodicl1lorometl1ane Dibromome!hane cis-1,3-Dichloropropene lrans-1, 3-Dichloropropene 1.1.2-Trich!oroe!hane lelrachloroelhene 1.3-Dichloropropane DibromochloromeU1ane 1,2-Dibromoetlmne Chlorobenzene 1, 1. 1,2-Telrachloroethane Bromoform 1, 1,2.2-Telrachloroetliane large! Ouanlitalion Umil-Subject lo change due to instrument sensitivity renlativety Identified, not conlirmed Estimated Value 0.75 10 0.75 0.25 0.25 0.25 0,25 0.75 0,75 0.25 0 75 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.75 I 0.25 0.25 0.5 0.75 U-Samples analyzed for lhis compound but nol delecled N-Sample nol analyzed for tills compound 0-Detected below quanlilalion limit M-GCIMS Analysis performed COMMENTS: 1:1 ltlH/llW{.) 1,/\IIOHI\ IOHY VOi.A Ill.I'. MMI.Y I ICAI. Hl;l'{lll I Ul:IH:11,:1i II. 0.59 0 46 3!'1 E 3.0 1.0 II II II II II II II II u II IJ u I) u u u IJ II u u u u !IG-18-4 108-BG-1 !J~-49-B 106-43-4 5,11-7J-I 106-46-7 95-50-1 96-17.-8 1/0-117-1 8 7-68-3 87-G 1-6 1634-04-4 71-43-2 108-88-3 100-41-4 108-38-3 95-4 7-6 100-42-5 98-82-8 103-65-1 108-67-8 98-06-6 95-63-6 135-98-8 99-87-6 104-51-8 91-20-3 ··-••·•··. ····-.... ••--· VlJA lAIHil:,l'Cl,lMl'tH/tlll 1,7.3-1 riclilnroprnp;111e nrm11nben1r.11e 7..(:t11<1rn!oh1r.111i 4-Ch101nln!ur.110 1.3-1 Jict,loroh(?111.er10 I. 4-Dic:11lorohen1enr. 1. 2 -I lid 1/or nl>r.r11,~r11i 1 .?:-1 lil unmn-3 -(:I 1lnrnpr111><1IHJ 1.7.•1-11ir:l1l111nll\!lll!?IIIJ I !e~;ichlnrob11t<1diene 1.2.3-1 rir:hloroben1e11e t,1elhyt-lert-butyt e1her l]e11zene r o!uene Ethyl benzene rn.p-Xylenes a-Xylene Styrene lsopropylbenzene n-Propylbenzene 1.3,5-rrime1hylbenzene te1I-Bu1ylbenzene 1.2.4-1 rime1hylbenzene sec-Bu1ylbenzene p-isopropylloluene n-fJulylbenzene Naph1halene Gasoline Range Estimated Total Pe1roleurn I lydrocarbon OIiier purgeables de!ected (up to 10 highest peaks) I.All tHl. Tlt(llfll o 25 0 ?5 n 25 O 25 0,, 0 2'.i O 25 0 75 mgll 5 I I 2 0 25 0 71 I) mg/L Detected ugll 11 11 II II u 11 11 II 11 11 u u u u u u u u LI 11 u u u 11 u N ------------------------------------------------------------------- D I I I I I I I I I REFERENCE 21 · I I I I I I I I I I /\;/ q_/ !·'!) I· I (?/\'~ ri/"/S \-,,,m-7. ·v--io_:m_,r·--:J ('IO!j,1'.)0F" . -l -;.,,;, p,-.y;, (!)- iiiil ----- . ~ ?<;,Jdc'?L"h']--➔vii r- • • I 1--- ])loz{ft!i"?PnFP:l---?!J.d:'s !,"1uoN1,-: j;l,-p?n/ld- i I : u,CJ.!j)Jdn11 J•>-v?;11chpi1,p psv:x ----;V:vi_c~1<_9-;'/r - i-:__, \ ________ : ------1--- ! r-~v ,j ·'?:/ v.-_,, ---l!!!!!!!!!!l l!!!!!!I l!!!!!!I == ; i ·--'j I I ' . : - I I i {l;-ll\i -j ,. C ! _ f---c,--~---~-o-, ,,__u,_"<L.L! -- ;,s iiiil liiil -5('JQ1:i.:f1¢1 ""1l-'l'll'z;·7;· ·:w_-i;;;r--- - -,:,.,__ _, __ , .'.~, :.,? (1 ~<JC I 1 @ (lcJ_ H-t ·]I:!_ r7 0·• Ci r ·- I ! L-''·1b <:',·.'Cl.' ® C!<{ :-n J:J~1 ' /' C[({ ~--- s: ---z..c ; i'1---zJ -- .. 7: ~D c,J,:.'/ I ;/0) '--c/ C!J i-n ·~;J., /' SI Ii I -J 1, (, J J !~ ' :c I -·:--i (0 I CJ. 1,-/1. ~;-'%!, ,.., /1 O' i I ] I crz.;J_t --!---r·· ?. -·· 1--·-· 1 -;; -------I -··1-··· I I ,,-.--z 7. -z---;- -:J! Ol . -l-1iO(~ /, {,/ I ! ·:sl, I Tl rl) qJ ?f) -·--® -\'}wow u.r/>J /-17 '!;>;,J 'l,-J7(iJ 't1'1 -W1 1'~J'i<;c'JTIVN~-. .c, I ~ . ,-,_-,;, ------... ; · 1 /1 -amlY'/2:DUJt~ I ' ' ' ------..--------I / /1: ' , Jt)J~rrra: c;, JI -~-_ c,£'f,O «fr;o· --,,£LI [ -ot'':lr! ~ar·s;r'--.:,w1_:c ---_____::.CL.-. .c::....._ _ _;_· 'Z yil1, --i./ J,,;3, -hh/·r1· 8-:~,1·1c-lc---·----,, ,,c.--· ,> ,r1 · N-re! P1 -t-J :,+,...,,:!:;~.-ta ,_-c, ,~ -_:: .. 1 !-,::,::~-l----s:-~crl1 :: _:-:_-] 1~:u -_---_ ... .._. "-'· -J) ":'1 _1 ---C -,__,. ,___. _ c.. --, -- - -----___ ::------ - - I' : '' .✓ L: .. /.W \<6 U1 : 1<G,I.H, 9\1:<Pus:R<, .... __ :pG. . --:ro - {,,o,,»udi . @ . @ 0~1e,'-I" I 120"! 1-I I ,-z_. I _ I -\_ .. I -1 1- -! -·-·"-~'~( )o· i:-----. ,.:: -l -'.( -,-- ·I)_..,.,·). /_,J~/'1L/J - - --- - - - - - I• I' I i '. - - --- - -·.--- r -------- 1 · J?'/"i}Hl')J'°Y)q 11 ! {/-~ V , b{'J:;,,,~?J.UJ:J' '!1/.f 11'\VJ I . }71,<0) Tiff /0 I I J , , .,..,-9rfr-l "If 117W/ 9 ,J?,p · ,?w nJ0 .;r --- .;7,,,r,;J ?ct 01 If J?i•f/ ,1ia-:; y,;.f??J/PJ ;>t/ 'j,J,1 y,p?,;;_, 7(1..-,,??f 1&v,11s fl : ·p· .-,,:-.~1·y1np/,:i?brv" 1.1,J ?n))i,J , . , .~ v If. :>/?' lj./-, Vi4(.''? )7 J'>,?,11.>} )7//1'-'~ 1/(')19_/g '(?,?-(} I , I 'I /I. Jryvb,,., 'r,_;('1 Ci :. )71<,<}./ . ,'1-!d 'v"'.I) i,,,0n?!M ,;r.1_ 1f· C ., i \" :,~v1'17j' ,r-t/ · ·1.Y-p~t" -r;n-,?) Pi?YI (YJ · Q( d . ~.:i11v::oy >01 j;,;,, "'17.f ._, 01 fj. p11..x) '""!/ '"'i'.:/ :, . ,;:,_,,,u<; ;711:yn CJ n,m ~ I <Ji:) - I:. I • ,3 I ·J;l ;- ~ ~\ -I S' 0 0 t "" :-r f I I~ *~ ' j ~ --" :0,--,, -__J l j . ' I J ~ o.l SL tJ ~ --q j u ' ~ ' ...::J ~ I ~ j cl Q' v':l ----" <' . .'\)! ~ ~1 J ,. ' I'- 'C w 1· -.5J 1,. ~ 'C, t "' .,; r.., ' ~ t v 0 ·--e I "'-- I '""' "' -'-ri -L " ,~~i11? /}i'' < ·,-:'t /ii} .:J :;;:! { ';,'.~= -'1 /. •::,..~ ,:, ;~-; \r' j --· - - -- --··-'J/ ,: ... , \\~. 1, £{: 2 .:i r1. I;', rev,r tr m ,. L s V -. 2 I tl,,A "'"'''"-"1L--+==L_-'--l~p:!ve~,e~v.'cvt~_1.,;,µNb lb ii L z he.,. I 11,'h I 'i,•I 1-it""'-'1'--'-'-'-+---+----+---l-----l------l----+---+--..j_-+-~--1----1---.,----'.- r-~~-t----1----+------f---1-----1 ---~1-----+---i<r+-----+----+-=7==---- r q -:,_._,__._,__.\-d-l----+-----1-------1------l-----l ;; I I I ---!~- I I I I I •. : I i I ,: ·cf q ,., ·_;:: G ' I ,~,. ----,--- \'-,. ' --·--'-'.-! ! ::...1 o, -a "ii -91 COMMERCIAL • RESIDENTIAL • INDUSTRIAL N.C. General Contractor"s Lie No. 25112 704-528-6192 .............._ Built Ups • Shingles • Single Ply• Insurance Claims • Estimates Gladly Given Post Office Box 5602 Statesville, NC 28677 • I lcnlth, & Natural Resources N c. Department or Envuonment, ~ SAMPLE ANALYSIS REQ{JEST Solid Waste Management Division A( State Laboratory of Public Heallh P.O. Box 28047, 306 N. Wilmington Slrcet Raleigh, North Carolina 27611 ~ u, l -\itc Number _________________ Field Sample Number ___ .!.C/,:.0__,/'--7.,__ ___________ _ __ Name of SitcS,')\\'l!hl 5epbc/AA.4 cal::up(1\u Site Location._~P<::=i"""--"''Q"'--------------I I I I I I I I I I I Collccted By(1l0,;,r /r--(6.fb'-" (hy,t.,_ ID# i-·, /,..i/1, Date Collected 'i'/1 /Jv Time / 3 3c I I j ------------------ Agcnc)C _h_Hazardous Waste Solid Waste _· __ Superfund TCLP Compounds Sample Type Environmental Concentrate Comments _ Solid (5) , . , ..... , .. , __ Ground water (1) __ Surface water (2) _ Soil (3) £ Liquid (6) -----·-'-· -'------ Sludge (7) _______ ,_._·-:.--=--- 1 l 1 _I .... _ .• _ Other (4) _ Other (8) Organic Chemistry Inorganic Chemistry Parameter _ P&T:GC/MS _ Acid:B/N Ext. Results(mg/1) Parameter / Arsenic ✓ Barium Results(mg/1)~ <'..o,o'.:\ l\!TBE ~ Cadmium Chloride _L__ Chromium __ Copper Fluoride Iron ./ Lead Manganese 1./Mercury Nitrate L Selenium r------------------s v Silver Radiochemistry Sulfates ······-··--------------..; Zinc 0, 8 8 0-C,.::}_ \ Inorganic Compounds Arsenic Barium --Cadmium --Chromium --Lead ----Mercury Selenium Silver Organic Compounds benzene --carbon tetrachloride --chlordane --chlorobenzene --chloroform --o-cresol --m-cresol __ p-cresol cresol ----1,4-dichlorobenzene __ 1,2-dichloroethane __ 1,1-dichloroethylene __ 2,4-dinitrotoluene __ heptachlor hexachlorobenzene hexachlorobutadiene Results(mg/1) Results(mg/1) I I ---------- I I Parameter __ Gross Alpha Gross Beta Results (PCi/1) Microbiology Parameter Results (Col/l00ml) _pH __ Conductivity TDS --TOC hexachlorocthane __ methyl ethyl ketone nitrobenzene pentachlorophenol = pyridine __ tetrachloroethylene trichloroethylene = 2,4,5-trichlorophenol __ 2,4,6-trichlorophenol I __ __ = vinyl chloride :1 ..... :. .. :•··· ·· -·· · · · · .. . .... ,. . . --~~~:i~e I [)ate Rc_ccivcd_,_·_···_·_-_--_. _··_--··_-_._-_•._··_··_·····Rtpciitfa°by_'_-_· -_--_·_--_··_. -_ .. _._ ... _-_··_·_· _._ .. _::_.·"_·' ;_. ·=·iiiethoxychlor ., - ) __ toxaphene . Dote Extracted _________ Date Reported._________ __ 2,4-D I _ 2,4,5-TP (Silvex) Dote Analyled Lab Number -~------------------ --1 ' _______ , ! ------- I N.C. Department or Environment, SAMPLE ANALYSIS REQUEST I icallh, & Nalura\ Resources I : · Solid Wasle Management Divisio.n 7, State Laboratory of Public Health P.O. Box 2&047, 306 N. Wilmington Street Raleigh, Nonh Carolina 27611 Field Sample Number ___ q,__0"-"'()'-9,__ _________ _ I I I I I I I I I I I I I I Sile Number ________________ _ Collected By (f/,v,u /t-1w+(.,,. , Site Localion __ ...,f.._,-"u'"/4-t'-"-'-'Q....=-------------- Dale Collected __ li;'4-/=-Jc;/ /'-z'-'2,"------Time_,_/7:,,.J,,.6"--- Agency: ___:i_ Hazardous Waste Solid Waste _· __ Superfund TCLP Compounds --- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium "P7 -kl -- Ground water (1) _ Solid (5) Cadmium --Chromium -- _j,_ Surface water (2) Liquid (6) Lead ----Mercury . Soil (3) Sludge (7) Selenium --Silver -- _ Other (4) _ Other (8) ---- -- Organic Chemistry Inorganic Chemistry -- Parameter Results(rng/1) P'lrnmeter Results(mg/1\(J.lp (I Jt,-Organic Compounds Results(mg/1) --P&T:GC/MS -./ Arsenic ,;(_ C -0'::1 benzene ---- --Acid:B/N Ext, ...L Barium (),Q-C carbon lelrachloride -- MTBE _i_ Cadmium -"--Q • a \ '-"-chlordane --J,:;' -- --✓ Chloride chlorobenzene -- --v Chromium L.., o_ o::J chloroform -- --__L. Copper {o. o,c o-cresol --, e rn-cresol ------, JrooJI __ p-cresol ---- --...L Lead L.... 0-Q:jD cresol -- --~ Manganese I)< '.2± --1,4-dichlorobenzene --_;'.'._ Mercury L..o. coad. --1,2-dichloroethane --v Nitrate ( 7,oo __ 1,1-dichloroethylene --._,/ Selenium -"--0 -Q ':l 2,4-dinitrotoluene -- ..L,__ Silver L. o. a":, __ heptachlor Radiochemistry _L_ Sulfates L. L,_ hexachlorobenzene --.... ________ __1LZinc <o. o C hexachlorobutadiene -- Parnmt:ter Results (PCi/1) _!'.'.,_pH '1.0 hexachloroethane __ Gruss Alpha _:!_ Conductivity ::\l<i'::i.,,~ __ methyl ethyl ketone Gross Bela _e_ iii 0 I nitrobenzene ----penlachlorophenol _iL TOC /Srvip ,_.. -' + de.('~ __ pyridine -- Microbiology ----tetrachloroethylene --__ trichloroelhylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride --en_drin lindanc c-;si)"a'tc~R-cceivea',;,;,;,:,:_;~,.a,,<::.·.c_,•.>,_,:, -- --.... -Reported--by,,,,~:-----. · .... -.. ... _._ .. _, 111'-thorychlor .. . -,-, ........ •·· --~- ,, . ... .-... __ toxaphene ci ,;i C. Ext racicJ Date Reported 2,4-D __ 2,4,5-TP (Silvex) Dale Analytcd Lab Number -- 1\11<.: 11<)\ (11,-vis:,-d 1/l}l) --------. -- i I I ! , I SAMPLE ANALYSIS REQUEST N.C. Department of Environment, · 1 lcalth, & Nalural Resources 1 · Solid Wasle Management Division 7, State Laboratory of ?uolic Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 I I I I I I I I I I I I I I ·:ite Number ________________ _ Field Sample Number qO 0 ----'=--'-"------------- _Name of Site/);r)Wf?Yl f.lpf1c /4fif± Or!«pn ',(_,J Site Location __ ~E.=u.,,w,.,,_..,a""~'--------------- Collected By &ic,s.,:/ Ma.m"' I Dqo '"-ID# 1~6 '1 /q , 1 I Date Collected __ ..1.J.f./-'-1.f./_'fu,z.,,e::_ ____ Time_"-0.,__7.c..:i.--=o'---- Agency: _L Hazardous Waste Solid Waste __ Superfund Sample Type Environmental Concentrate Comments __ Ground water (1) _i_ Surface water (2) Soil (3) _ Solid (5) _ Liquid (6) __________ _ _ Sludge (T) __________ _ _ Other (4) _ Other (8) Organic Chemistry Parameter Results(mg/1) _ P&T:GC/MS . __ Acid:B/N Ext. MTBE Inorganic Chemistry Parameter ../ Arsenic Results(mg/1~ ~~ <-C>-0::\ ✓ Barium ✓ Cadmium ...J!._ Chloride \/ Chromium _:/_ Copper :1 Flnwi:tk _s{_I sa ..Jl..Lead cl Manganese v' Mercury _..lL_. Nitrate .Jc'._ Selenium Q, 2(, 13 0-17: D, <./ b t----------------l _LL Silver .<:. o-oS Radiochemistry ✓ Sulfates "1, ······-··------------1 _iL Zinc 0, f'.c) ParJ.mdcr __ Gross Alpha Gross Beta Results (PCi/1) ✓ pH /.g , :-J v Conductivity 'I c.. Q ,-.,,,, 2 .,... _J£_ ID fjlt ___ 1 ___ _ f-----------------1 _i.l TOC ef"'p~•-f-.£,0 '- Microbiology Parameter Results (Col/lOOml) Dote Extroctcd _________ Date Reported ________ _ Dote Analyzed Lab Number ------------------ TCLP Compounds Inorganic Compounds Arsenic Barium --Cadmium --Chromium --Lead --__ Mercury Selenium Silver Organic Compounds benzene --carbon tetrachloride Results(mg/1) Results(mg/1) --------- -- chlordane chlorobenzene chloroform o-cresol m-cresol __ p-crcsol cresol __ 1,4-dichlorobenzene 1,2-dichloroethane __ 1,1-dichlorocthylene ______ _ __ 2,4-dinitrotolucne __ heptachlor hexachlorobenzene hexachlorobutadiene --------- hexachloroethane __ methyl ethyl ketone nitrobenz.ene __ pentachlorophenol __ pyridine __ tetrachloroethylene __ trichloroethylene __ 2,4,5-trichlorophenol __ 2,4,6-trichlorophenol __ vinyl chloride etldrin lindane · ·~ inethoxychlor __ toxaphene 2,4-D __ 2,4,5-TP (Silvex) -------' ' _______ , _______ ! _______ : I I I I I I I I I I I I I I I I I I I N.C. Dcpanment of Environment, , llcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 -.. '.~itc Number _______________ _ Field Sample Number __ ---'-}"'6'-'-'/ 3""'---------- Name of Sitc-;i'r'M' ~ip:h l ,ffifl,f-:s i;:l\t<Ypn',l,\ -~ollected By G-(&~( //1[.J.r-. /Dtqry,.. ID#\7/14/1 I F I r I Site Location f ½-h2{a__ Date Collected Cf /1 / yz, ri Time JO/":! Agency: 1-Hazardous Waste Solid Waste __ SuperP.lild TCLP Compounds -- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- 74-w Barium -- __ Ground water (1) _ Solid (5) Cadmium --Chromium -- .]{_ Surface water (2) _ Liquid (6) Lead ----Mercury _ Soil (3) _ Sludge (7) Selenium --Silver -- _ Other (4) _ Other (8) -- -- -- Organic Chemistry Inorganic Chemistry -- Parumeter Results(mg/1) Parameter Results(mg/1)(~ Organic Compounds Results(mg/1) P&T:GC/MS ./ Arsenic ..c_ o,o':\ benzene ------ Acid:B/N Ext. v Barium O,U'J,. carbon tetrachloride -- _L Cadmium MTBE L...O_Q\\9 chlordane ---- --_kc_ Chloride 99 chlorobenzene -- --2'.-Chromium L..o -o'-+ chloroform -- --~ Copper c2 . ;;i 8 o-cresol -- I. Fl: Pde m-cresol ---__ p-cresol -- --_iL_Lead a "a <otf cresol -- --_L Manganese z, 7---1,4-dichlorobenzene --_L Mercury L.... o_ a s:;i<::>-;}.. __ 1,2-dichloroethane ----lL Nitrate < /. De) __ 1,1-dichloroethylene _L Selenium L.c,.i;i '.:l 2,4-dinitrotol uene _.,J_ Silver 4-0.QC::, __ heptachlor Radiochemistry v Sulfates L_ \ ')... hexachlorobenzene --/, 08 --... , .. _.,_ ' Zinc hexachlorobutadiene ...:,L -- Paramt:ler Results (PCi/1) _,l._ pH '-'>-:'.] hexachloroethane __ Gross Alpha ✓ Conductivity 1 3;:;bQ, .:::o:::s-__ methyl ethyl ketone Gross Beta iJiE □• ' 7 nitrobenzene • ----_L TOC Eyvy.,-•~+-c(, si·"" __ pentachlorophenol --__ pyridine . Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophcnol -- --__ 2,4,6-trichlorophenol -- ----__ vinyl chloride endrin -- -~-"r:)·,;1~~ R_-g~Ei ~~~~.::,,;;. ---· lindane _.,, .. . ··--··· '··•-"= ·,::.R:e ported: by>:/s=:0 -. .. ;. ~,:.. ·:----.: .,.,.s:-0 m'ethoxychlor . .. . ···-· -' .. toxaphene -- D~1\c Exlractc<l Date Reported ·2,4-D _ 2,4,5-TP (Silvex) Dale Analyzed Lab Number -- ""'-~""'"-. --' .. ,,,, ~ I ' I N.C. Department of Environment, SAMPLE ANALYSIS REQUEST . , I k:ilth, & Natural Resources I Solid Waste Management Division State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 -~' . ~itc Number _______________ _ I __ Name of Site >tgm,n1 xr/ic-,IABA: ir(erpni,u Field Sample Number __ .....;.o/o.;__· ..:.i..=5c_.. _________ _ Site Location __ -'g_.fv==/c..,:;... ______________ _ I I I I I I I I I I I 11 Collected BvG/o. ',/!slrtwti r./p~(/'\, ID# 13./1~/11 Date Collected __ '/'-'/_1..,/c....:.?_-i---_____ Time_/'--'--1..c(.,:Oe:_ __ Agency: -1.._Hazardous Waste Solid Waste __ Superfund TCLP Compounds -- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium Ground water (1) ?;3 ,w --Cadmium _ Solid (5) --Chromium -- ...:L_ Surface water (2) _ Liquid (6) Lead ----Mercury _ Soil (3) _ Sludge (1) Selenium --Silver -- _ Other (4) _ Other (8) ---- -- Organic Chemistry Inorganic Chemistry -- Parameter Resulls(mg/1) Parameter Results(mg/') (g;ia.'.i~ Organic Compounds Results(mg/1) P&T:GC/MS , Arsenic L.. o_c,'t benzene --_,,_ -- Acid:B/N Ext. ~Barium 3, C9 carbon tetrachloride ---- MTBE V Cadmium 0-13\ chlordane --__iL Chloride L(Lj -- -- chlorobenzene -- --_!::'._ Chromium o .. a,S chloroform -- --~ Copper /, S-0 o-cresol -- --1,-= Fl BUI iek m-cresol Loa = p-cresol --- --✓ Lead .;J,-G9 cresol --/J,:JCi -- --~ Manganese --1,4-dichlorobenzene --..J::'.'._ Mercury L.o.co;,.._ 1,2-dichloroethane --✓ Nitrate s,_ /, 00 __ 1, 1-dichloroethylene ✓ Selenium £'.. 0--'-'r 2,4-dinit rotol uene _L Silver .L.. o. o':J. __ heptachlor Radiochemistry v Sulfates -""-(,,,0 hexachlorobenzene ---- ······-· v Zinc 1Y.Lfr hexachlorobu1adiene ---- ParJ.mt:lt:r Results (PCi/1) _JL__pH 5 :-"i hexachloroethane __ Gross Alpha ~ Conductivity 5 QC:Q q,:r::c,,2 ti __ methyl ethyl ketone Gross Beta ~ TSO T nitrobenzcne --JTOC Eyul/"I.Aol-.,,_+ d ,,.,_ ~ = pentachlorophenol __ pyridine --Microbiology --telrachloroethylene -- --__ trichloroethylene Paramt:tt:r Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin -- .. .. .. lindane .. •-·· ,·•:,· -·•--.• ·.' .. , .. .. . .. -. ·. , .. ··--··· . -- i I I I i i ' I I I I Date RccC:ivcd Rep6i1cd by __ riie.thoxychlor . ·-.-., __ toxaphene D:ilc Extr:,cte<l Date Reported 2,4-D ----2,4,5-TP (Silvex) Dale Analyzed Lab Number -- I N.C. Department or Environment, • \, I lcalth, & Natural Resources SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 I . .' Sulid Waste Management Division .... , 1Silc Number -----------------Field Sample Numbcr __ __,_ql}"'_.J:eD"'----------- I _Name of Site ◊-rqmM f.epbc /fM f;11-~eprl141 Collected By {;/c,:;gv/HCtd; n h;r,n.,-V\ ID# 1,/,~ / // r ' I Date Collected __ 'l'-'/_1'-l-/~1_v _____ Time____./""5'"·cc=--- I I I I I I I I I I I I I I I ' Agency: Hazardous Waste Solid Waste __ Superfund ------ Sample Type Environmental Concentrate Comments Ground water (1) _ Solid (5) £JD -I<\ X Surface water (2) _ Liqu.id (6) _ Soil (3) _ Sludge (7) Other (4) Other (8) Organic Chemistry Inorganic Chemistry Parameter Results(mg/1) Parameter Results(mg/1\~p (~ --P&T:GC/MS ✓ Arsenic ""-0 -st:\ Acid:B/N Ext. v Barium D. !o ---- MTBE ..L Cadmium L...o., O\i.....D. --✓ Chloride '.:)./ --/ Chromium Lo,e,'-\ -- --_L Copper < Q., oS- --_£_ Fl 'J --~ ---"--Lead L...0-C'oCl --..L Manganese !, o.r --_J:'.'._ Mercury L...o .. oc1~d-. --_,,!__ Nitrate ,(_ (, 00 _1L_ Selenium L...o.,c':\ V Silver .L..o.oS. Radiochemistry ..JL Sulfates ""--l...9.- ······-·· _!!_ Zinc 6, OS- ParJ.mctcr Results (PCi/1) ...JL.. pH <.s..S __ Gross Alpha _lL Conductivity \ 0 ~ C -~s:, Gross Beta .. +i!i'l" r --~ TOC £y-u 'f ..,..,.,_ ~ -(-d,,, W ~ -- Microbiology -- -- Parameter Results (Col/lOOml) -- ---- ---- Oat~;·Rc·ccivcd Reported by Dale ExtraeteJ Date Reported Dale Analyzed Lab Number !)11...; 11'J! (llcvi);cd 2/9\) ------~~ TCLP Compounds Inorganic Compounds Results(mg/1) Arsenic --Barium --Cadmium --Chromium --Lead ----Mercury Selenium --Silver ---- ---- -- Organic Compounds Results(mg/1) benzene --carbon tetrachloride --chlordane --chlorobenzene --chloroform --o-cresol --m-cresol __ p-cresol cresol --1,4-dichlorobenzene --1,2-dichloroethane __ 1,1-dichloroethylene 2,4-dinitrotoluene --__ heptachlor hexachlorobenzene --hexachlorobutadiene --hexachloroethane -- --methyl ethyl ketone nitrobenzene __ pentachlorophenol __ pyridine --t e tr achloroeth yle.ne __ trichloroethylene __ 2,4,5-trichlorophenol __ 2,4,6-trichlorophenol __ vinyl chloride cndrin --lindane __ . methoxychlor __ toxaphene ' 2,'1-D = 2,4,5-TP (Silvex) -- I ' ' i I I •-- I I I I I I I I I I T-Jcalth, & Natural Resources ~ ;;.....) <---'~ State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, Nonh Carolina 27611 N.C Department of Environment~ SAMPLE AN.' .. LYSIS REQUEST Sot,d, Waste Management D,v,s,o U\ t Site Number __ _,_ ___________ Field Sample Number __ _,,_,/,'--'/C-"/--'-z',-"'L~-------- Sile Location ('u rOL 6f= Collected By u.k/.<" /4 -w ID# /f/%V Date Collectc_d 8'.5/f'z_ Time (._S:,?g_ I -~ ,.--, ·:·. r" (..,, r:-! ', ! . , {" TCLP Compounds Agency: J zardous Waste_·:·_._•_._· Solid Waste __ Superfund Sample Type uCi Li [ 19c? Inorganic Compounds Results(mg/1) J Environmental Concentrate Comments Arsenic -,;i; r_;·r_ i ((:j\l~;J --_ s;1;ci cs>_:y Barium ·" -P~c;{J --__ Ground water (I) Cadmium --Chromium __ Surface water (2) VLiquid (6) --Lead -- --Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) ------Organic Chemistry Inorganic Chemistry -- Pararnckr Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) d!&T:GC/MS Arsenic benzene }:2'Acid:B/N Ext. ----Barium car!.mn tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobcnzcnc ------Chromium chloroform --------__ Copper o-crcsol --Fluoride m-crcsol ------Iron __ p-eresol --Lead crcsol ----------Manganese 1,4-dichlorobcnzenc ----__ Mercury 1,2-dichloroethanc --Nitrate __ 1, 1-dichloroethylcne --Selenium 2,4-din it rotolucne --Silver __ hcptachlor --Radiochemistr)' --Sulfates hcxachlorobcnzcnc --····-·····--···-·--···---···------····-··--·-·----·······-··-· Zinc hcxachlorohutadicnc '-----1'~1rametcr Results (l'Ci/1) _pH hcxachlorocthane __ Gross Alph;_i __ Conductivity = methyl ethyl ketone Gross Beta TDS nilrobcnzcne ----TOC __ pcntachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylen_e --__ triehlorocthylcne Paramtter Results (Col/I 00ml) __ 2,4,5-trichlorophenol ------__ 2,4,6-trichlorophenol ----__ vinyl chloride cndrin --6'2 ,D SEP 2 !992 /,) ?-lindanc O;dc Rcccivcd -P = mcthoxychlor Reported I,_ / __ t'.ixaphcnl'. -· I I I -1---, . '• ,,_ D1-E_1_ 11/(/91--i/1.f ··-!;,;;, :1 C.; X G1c(C( · ... ,:-~.-'.. . , .. : ... :~....;. ___ Diilc·Rc·ji,~-· "/tJ-j-'f~ 2,4°D .... ·-:, .. -:-.--------·;: .. :. ---.,-·-----I --fJ.JA pr ,--~:-,··,-·, .--..r4 2,4,5-TI' (Silvcx) Dale Analy1.cd 9-dyJ-9-/!t9:J Lah Number :,.-~,_;_,::,•c.;;. ... _. --C:l'IJR'il' 6&-'JU}J I I I I I I I I I I I I I I I I I I ! c-:.~:. Department of Environment, Health, & Natural Resources Solid· Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number -----------------Field Sample Numbcr __ ...,./'-'1/,'-'/--'--7_,,.77~--------- Site Location. __ :::Clc.:l{::.L.r,_,(J=LLc(l-"'-------------- Collected By u£?Sff /4~::?/V JD#~ Date Collected 8/.3-/ /7 Z Time j{Zo / ,t)c, £//.,I /'( , , Agency: ~azardous Wast~ Solid Waste __ Supcrfund TCLP Compounds --- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --t--.t, :5 Barium --__ Ground water (!) _ Solid (5) Cadmium ' --Chromium --__ Surface water (2) Liquid (6) Lead -- / --Mercury Soil (3) // Sludge (7) Selenium ----Silver -- --Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Resulls(mg/1) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic ,/ benzene LL. ----Acid:B/N Ext. Barium ,/ carbon tetrachloride ,J,-----MTBE Cadmium ..JL.. chlordane ----Chloride J chlorobcnzcnc iJL-----Chromium V chloroform o,OQ,?, 3, 2, ---- --__ Copper V o•crcsol Fluoride (/ m-crcsol ----V p-crcsol Iron ----Lead v crcsol ---- -----Manganese v 1,4-Jichlorobcnzcne Mercury v 1,2•dichlorocthanc . ' ---- --Nitrate ..iL 1, 1-dichlorocthylcnc d,,. --Selenium ,_,-" 2,4-dinitrololucne --Silver ~ hcptachlor --Radiochemistry Sulfates V hexachlorobcnzenc --.................. . ·-· .. -.. -.. ·-·-· ··-----·· ....... -· ·-·--···· ······· ... Zinc ..iL hexachlorohutadicne --l'ar..tml'kr Results (l'Ci/1) --pH ~ hexaehlorocthanc --Gross Alpha --Conductivity -~methyl ethyl ketone Q.Ql5 Gross Beta TDS ...L::'.'.' nitrobcnzcnc ----TOC .LL pcntachlorophcnol --V pyridine --l\·1 icrobiology --1,,/ tetrachlorocthylcne L.L ~ trichlorocthylene -· ' --Parameter Results (Col/lO0ml) --v' 2,4,5-trichlorophcnol ----v 2,4,6-trichlorophcnol ----_JL vinyl chloride I I ~ cndrin SEP 2 E92 f.,V . ./ lind;rnc Dale Received --Reported by / methoxyehlor ·•""'iY!lf c·· Efh:ftttJ:~fi-1t':'"'7":E-,oi3'•,.,~~-,~:_.7 n~\c .·P\: p~)! t·cd --· L,, .. tox~p~cnc . -J 2:4:0 . ·-• : ... ':")J:,Ji{ ··:"pr -:_· ,,. ;. ~-·_,,, .(1, ,.., / ) ,/ 2,4,5-Tf' (Silvcx) Date Analyzc<l1-/ t(-'iJ-9-t'+:9,) Lah Number .. J . .,,v,_]J\ ... --C:l'DR1JE /JiJJ. -tW,~ - I I I I I I I I I I I I I I I I 1-- 1 ' .. ~, Department of Environment, I 1·callh, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST ' State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, Nonh Carolina 27611 Site Number ________________ _ Field Sample Number __ _,__/,L/.,__/-'-'7..,,6"--------- Name of Site .,J'/t'---/Y0"7 ..f,E/'flc/4,a -FNT"° Site Location_-"'E,'-"-cr'--'/2'----"'o,:.=4-'---'-____________ _ Collected By fu ££"7/4~ ID#-#---Date Collcctcd_-----'!3,"tf /2~'.3'._f~/,,,__/5_9_2-___ Time_~/~7:--"~--"0"---- Agcncy: ~azardous Waste ___ Solid Waste ___ Supcrfun<l TCLP Compounds ! Sample Type Environmental Concentrate Comments Ground water (1) brr ace wate, (2) _ Soil (J) _Solid (5) __ Liquid (6) ___________ _ _ Sludge (7) __________ _ _ Other (4) _ Other (8) Organic Chemistry Paramt'ler 1/ P&T:GC/MS _""°v7_ Acid:B/N Ext. Results(mg/1) MTBE Radiochemistry Par.Hul'lcr Hcsults (PCi/1) __ Gross Alpha -------Cross Beta Microbiology Par.imder Results (Col/1001111) Inorganic Chemistry Parameter Arsenic Barium --Cadmium --Chloride Chromium -- --Copper -- Fluoride Iron Lead Results (mg/l)(mg/kg) __ Mang~incsc __ Mercury Nilrnlc Selenium -- Silver --Sulfates Zinc --_pll __ Conductivity TlJS TOC Inorganic Compounds Arsenic --Barium --Cadmium Chromium -- Lead __ Mercury Selenium --Silver Organic Compounds benzene --carbon tetrachloride Results(mg/1) Results(mg/1) ---------chlordane --chlorobcnzcnc --chloroform --o-crcsol --m-crcsol -- --p-crcsol crcsol --1,4-dichlorobcnzenc --1,2-dichluroethanc -- --I, 1-dichloroethylcne 2,4-din it rotolucne -- --hcptachlor hcxachlorobcnzcnc --hcxachlorohutad icne --hcxachlorocthanc ----methyl ethyl ketone nitrobcnzcne ----pentachlorophcnol __ pyridine __ tctrachloroethylcne __ trichloroethylenc __ 2,4,5-trichlorophenol __ 2,4,6-trichlorophenol __ ,inyl chloride I I I I I I I I I I I I I I I I I I I N.C. Department of Environment, llcalth, & Natural Resources Soiid Waste Management Division :::itate Laboratory ot Public Health P.O. Box 28047, 306 Jo. Wilmington Street Raleigh, Nurth Carolina 27611 Site Number _______________ _ Field Sample Number // / 9? -----~~---------- Name of Site Collected By ,.f/f:l'tcw~/4M E,,/;. Site Location _ _,,!5'-"'cr-'-A-"-tJ_L--'-,4-q-___________ _ U4St(i/4,4 t€.?7,v ID##.-Date Collected 1:¢ 2-Time 09ZO ----"----'---_..c;_ __ ..?'o /i? /V /I Agency: VHazard9us Waste Solid Waste ___ Superfund TCLP Compounds --- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- f-,Stv Barium --__ Groundwater (!) _ Solid (5) Cadmium --Chromium ..JL.. Surface water (2) --_ Liquid (6) Lead --__ Mercury _ Soil (1) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) . V P&T:GC/MS Arsenic benzene ----__iL_ Acid:B/N Ext. Barium carbon tetrachloride -----MTBE Cadmium chlordane ------Chloride ch!orobcnzcnc ------Chromium chloroform ------ --Copper o-crcsol ----Fluoride rn-crcsol ------Iron p-crcsol ------Lead ere sol ------ ----Manganese 1,4-dichlorobcnzcnc -- ----Mercury --1,2-dichlorocthanc --Nitrate __ 1, 1-dichlorocthylcnc --Selenium 2,4-dinit rotolucnc ----Silver hcplachlor ----Radiochemistry Sulfates hcxachlorobcnzcnc ----.... .......... ··········-··-···-·-····-----···-··-··-·--·····•·-..... Zinc hexachlorohutadiene ----l'araml'tL'r Results (PCi/1) _pH hcxachloroclhanc --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobcnzcnc ----TOC __ pcnlachlorophcnol -- ----pyridine Microbiology --__ tclrachloroethylcne --__ trichlorocthylcnc Paramckr Results (Col/IO0ml) __ 2,4.5-lrichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ ,inyl chloride cn<lrin --6' SEP 2 !inJ:mc Date. RcccivcJ ?392 --Reported by --mct_hoxychl,1r _Dale_ Exl ra.eieJ .1/-lc/_:;h.s!) __ loxaphcnc ·--·•···· ))al_eJ,~p_ofled-.. ·,·.-~•--.· -... -:.:· --· ·;,_~:!?:~~:·::.:·:-·•·•.·-: :-.:. . .. (j,J;f f'1 --2,-l.S-TP (Silvex) -,. Dale AnalyzeJ f-1FJJ-']_-/':f_-'3_l Lah Number ,-. r; r -.,_ ,·:~ 3,.), --.~ . .-.·;c. ·.• .. -..: '-i, ' • '-·, •Jrol,-....,<....I • --• ... ,._ ., .. C:l'DR'JE IJ1.P --7U<r I I I I I I I I I I I I I I I I I I N.C. Department of Environment, Jfoalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina .27611 Site Number _______________ _ Field Sample Number_~/'--'-/---'-,,2---'-o--"O'---------- Site Location /z._.V/OL.# Collected By · ~/f'/4' / ,h,tf,e/--;:k' TD# t)~y' Date Colleeted r/5/92-Time {)f' .3S A> 12 ,v / ✓ r-,:c ,v~;;,; ()II 01 L , / Agency: ~rdous Waste ___ Solid Wasie __ Superfund TCLP Compounds Sample Type Inorganic Compounds Rcsults(mg/1) Environmental Concentrate Comments Arsenic -- fl-S's Barium --__ Ground waler (1) _. Solid (5) Cadmium --Chromium --__ Surface waler (2) _ Liquid (6) Lead -- __iL'siudgc (7) --Mercury _Soil (3) Selenium --Silver --Other ( 4) _ Other (8) ---- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (n.g/kg) Organic Compounds Results(mg/1) _ P&T:GC/MS Arsenic V benzene 0, 0 01-/ °J' --_ Acid:B/N Ext. Barium V carbon tetrachloride LL --MTBE Cadmium Vchlordane ------Chloride L/ chlorobcnzene 0 ol~' ----Vchloroform --Chromium o,!>03 :s, 0 -- ----Copper Vo-cresol Fluoride (_/ rn·crcsol ----Iron Vp-cresol ----Lead C-,/crcsol ----V 1,4-dichlorobenzene ----Manganc.sc ----Mercury V 1,2-dichloroethane u.__ --Nilralc V I, 1-dichloroethylcne J, --Selenium V 2,4-dinitrololuene --Silver --{_/ heptaehlor Radiochemistry --Sulfates L-/ncxac h lo robe nzc nc .............. ... ·········--··--·-------····-. ......... Zinc Vhexach lorohutadienc ----Parameter Results (l'Ci/1) _pH l/ hcxachloroclhane __ Gros.s Alpha __ Con<luclivily ~ methyl ethyl ketone Ll..- Gross Beta TDS ...1.L...... nilrobcnzcne ---- TOC __IL:__ pcntachlorophcnol -- --_L_. pyridine Microbiology --(,,/ telrachlorocthylene l-' ~ trichlorocthylcne :,./. --Parameter Results (Col/1001111) ~2,4,5-triehlorophenol -- ----__ 2,4,6-trichlorophenol ----,_,/ vinyl chloride I I. J..L endrin SEP 2 pj) c.,/ lin<l:rnc D:llc Received fl92 Reported by u ml'.thoxyc.:hlor 9-1 j' JJ-2..!]£) V \t>x:.1ph1.:nc ·· D:i1e·;Exl r:.1c!cJ 0.Jll'.. Rql<ldciJ·· --., . ,. " .. ~. ... , .. -... .. t-< 2,4'0--,0 :: . ··--_. . .. •- •' .. '·'---·-· .. -.·-, '·---: .... -· --.. -... ·.-.. , --·· ""': -::.·.: fy-,'/l-ff -r:. ~ ::----: .. c·i· 3 ... , {/ 2,4,S-TP (Silvex) ·"···· Date Anal)?.ed 01,;·,-·?J---2-L'::1_-q_;J___ Lah Numhcr ,.__/, d•V..__.. • l.) --C.':J'l)WJI; t:JJ) --nw---· -~ I I I I I I I I I I I I I I I I I N.C. Department of Environment, Ik,alth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilming1on Street Raleigh, North Carolina 27611 Site Number _______________ _ Field Sample Number __ ..!./,--'--':C,.Z"--'-"-'---------- 'Name of Site ,[/1('1(..)N ,.f)9?7(0,1-4 rf/'-'/. Site Location_~tfc.-c.;l.f:::l..L/:5-'<-0-'L"'N~------------F I ,gr Collected By &L,f$,f,7~';;i~,-J lD# 13;fr Date Collcctcd __ .c.77.,,_/4_,_/-1-jj_f_z._ ____ Time /,t(/015' Agency: ~azardous Waste ___ Solid Waste ___ Superfund Sample Type Environmental Concentrate Comments Ground water (1) __ Solid (5) /surface water (2) Liquid (6) ____________ _ _ Soil (3) _ Other (4) Sludge (7) __________ _ _ Other (8) Organic Chemistry Par~mt.'tcr V P&T:GC/MS V Acid:B/N Ext. MTBE Resulls(mg/1) Radiochemistry Parameter Results (l'Ci/1) __ Gross Alpha ______ _ Gross Bcl;_i Microbiology Paraml'ter Results (Col/l00ml) Inorganic Chemistry Parameter Resulls(mg/1) (mg/kg) Arsenic --Barium --Cadmium --Chloride --Chromium -- --Copper Fluoride --Iron --Lead --__ Manganese __ Mercury Nilralc --Selenium --Silver --Sulfates Zinc --_pH __ Conductivity TDS TOC TCLP Compounds Inorganic Compounds Arsenic Barium --Cadmium Chromium --Lead __ Mercury Selenium Silver Organic Compounds benzene carbon tetrachloride Resulls(mg/1) Results(mg/1) ---------ch I or d an c chlorobcnzcnc --chloroform o-crcsol --m-crcsol --p-cresol crcsol ----1,4-dichlorobcnzcnc ______ _ __ 1,2-dichlorocthane __ 1,1-dichlorocthylene ______ _ __ 2,4-dinitrotolucne __ heptachlor hcxachlorobcnzcnc --hcxachlorohutadicne ---------hcxachlorocthane --___ methyl ethyl ketone nitrobenzenc ----pcntachlorophenol __ pyridine __ tetrachloroethylene __ trichloroethylene __ 2,4,5-trichlorophenol ______ _ __ 2,4,6-trichlorophenol ______ _ __ vinyl chloride cndrin -- --lindone __ mcthoxychlor __ tox;_iphcnc __ 2,4-D __ 2,4,5-TI' (Silvcx) ' I I !· ·'·-·! I I I I I I I I I I I I I I I N.~. Department of Environment, 1-lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ________________ _ Field Sample Number __ ..,./--'/c...=:.02_,_·,-'z.:_=· _______ _ · Name of Site ...V&.lvtYv ~£1,?llC/4,4,4 Site Location 6q fc'[_l{f ---L::..:c..-J...ec..==------------- 4 / Collected By ~£~,c;llv ID# q;:fy': D ate Collected 7,/;, /9 L Time /o 2 6 ---'/7"-C,/,'--'-----I t),&J /I Agency: ~zardous Waste ___ Solid Waste ___ Superfund Sample Type Environmental Concentrate Comments _Groundwater(!) __ Solid (5) __ Surface water (2) _Soil (3) __ Liquid (6) ___________ _ ✓ Sludge (7) __________ _ _ Other (4) _ Other (8) ___________ _ Organic Chemistry Parameter _ P&T:GC/MS _ Acid:B/N Ext. MTBE Hcsults(mg/1) Radiochemistry l':iramctcr __ Gross Alpha Gross Beta Hcsults (l'Ci/1) Microbiology Parameter Hcsults (Col/lO0ml) Inorganic Chemistry Parameter Hesu Its (mg/l)(mg/kg) Arsenic --Barium --Cadmium --Chloride Chromium -- --Copper Fluoride Iron --Lead __ Manganese __ Mercury Nilralc --Selenium --Silver --Sulfates Zinc __ pH __ Con<luclivity TDS --TOC TCLP Compounds Inorganic Compounds Arsenic --Barium --Cadmium --Chromium --Lead -- --Mercury Selenium --Silver -- -- -- -- -- Hesulls(mg/1) Organic Compounds Results(mg/1) Vbcnzcnc ±coce- ,::7 carbon tetrachloride __ _,,'-'-e:.:· __ _ 7 chlordane v chlorobcnzcnc ~ chloroform v O·Crcsol V m·crcsol ~ p•crcsol V crcsol 0, 0 0 2\ :fLrc.'\c___ o.ooq ,3 VI ,4.dichlorobcnzenc L 1,2•dichlorocthanc (..L 1.,/'l, J .Jichlorocthylcne ___ .,J,'-,'--- V 2,4-dinitrotolucne ✓ hcptachlor (._,,/" hcxachlorobcnzcnc [,/ hexachlorohutadienc ______ _ ~ hexachlorocthane {./' methyl ethyl ketone ~ nitrobcnzcne ....f,Lpcntachlorophenol ~ pyridine e,/ tetrachloroethylcne ~ trichloroethylene £L.2,4,5•trichlorophenol .1L 2,4,6.trichlorophcnol .LL vinyl chloride 1,/"endrin I Dale Received SEP 2 '!J9t fjY Reported by__________ ~ ~:~t~~chlor ,";c·c~:-i5~I":'~i~:~?r::~!-:tz~~,-~·~ ~~:;i~.:~~~~~;;i~cd~~~ ~:-. : .. " ... ~ ..... -~ ·• ·r ~:':~~::l;Silvcx) I Dale Analyzed'J•/)-•1/). 9-1-/-9,2 Lah Number .~· · · ~- Cl'IJ8'1I' ,9 1' ,wr [;JTCLf' '{·30 -9;:/_ I I I I I I I I I I I I I I I I I ., N.C. Department of Environment, Health, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P .0. Box 28047, 306 N. Wilmington Street Raleigh, Nonh Carolina 27611 Site Number ________________ _ Field Sample Number ___ _,_//'--"..2.u~~3~-------- Name of Sile ,.f/tf.-/vW J/P?lC/41,4.4 tf{,.,;T, Site Location_-"'l'-;::-.::~'-'A_-..::c):...=L_,4.:,__ ___________ _ l Collcclcd By fi-<4,/f",C ffe,n;p.J / l ,Pt.,.Z/V ID# /_j!/v Date Collcclcd ___ -'1/+1/;-''/'-r'-/9~9'-'=z.=---Time __ /_/._/_o __ _ ~ Agency: .1L_ Hazardous Waste ___ Solid Waslc ___ Supcrfund Sample Type Environmental Concentrate Comments __ Ground water (l) __ Solid (5) i/2urface water (2) __ Liquid (6) ____________ _ _ Soil (3) _ Other (4) _ Sludge (7) __________ _ _ Other (8) Organic Chemistry Inorganic Chemistry Para;nclt:r Results(mg/1) Parameter Results(mg/l)(mg/kg) {/ P&T:GC/MS ✓A6J:B/N Ext. MTBE Radiochemistry l'aramcler __ Gross Alpha Gross Beta Results (l'Ci/1) Microbiology Paramdtr Results (Col/I00ml) -- -- -- Arsenic Barium Cadmium Chloriue Chromium --Copper -- Fluoride Iron Lead __ Manganese __ Mercury Nitrate Selenium --Silver -- Sulfates Zinc _pH __ ConduClivity TDS --TOC TCLP Compounds Inorganic Compounds Arsenic --Barium --Cadmium --Chromium --Lead -- --Mercury Selenium --Silver -- -- -- -- -- Organic Compounds benzene Results(mg/1) Results(mg/1) ----------carbon lclrachloridc ---------ch I or d an c chlorobcnzcnc --chloroform m•crcsol __ p-cresol crcsol ----1,4-dichlorobcnzcnc ______ _ __ 1,2-dichloroethane __ 1,1-dichloroethylene ______ _ 2,4•dinit rota! ucne __ heptachlor hcxachlorobcnzcnc --hcxach lorohutadiene ---------hcxachloroclhane __ methyl ethyl ketone nilrobcnzcnc ----pcntachlorophenol __ pyridine __ tetrachloroethylene __ trichloroethylene __ 2,4,5-trichlorophcnol __ 2,4,6-trichlorophenol __ vinyl chloride -- cntlrin lintlanc --mcthoxychlor I I I I I I I I I I I I I --I,,, I I I I I N.C, Department of Environment, licallh, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number ________________ _ Field Sample Numbcr ____ LC.../.c.J_:_c>+--------- Name of Site ,.f/{.hMJ,-[',,f:?t,7C /1-1,0-;I £-vT, Site Location. __ -"E~-...=.,..,,r_-c.c)_Lr-'-,4",-------------- Collccled By i(l~<,/1/-Y -?/2,v ID#~ Dale Collccted __ -'-~-l-/-'-(,+'/--'-7--'z__=---Time / / / 5 / /?1:,,t!,v / I Agency: 0lazardous Waslc ___ Solid Waste ___ Supcrfund Sample Type Environmental Concentrate Comments __ Ground waler (1) _ Solid (5) P-3S __ Surface waler (2) _ Liquid (6) __________ _ _ Soil (:l) _ Olhcr (4) _ Other (8) Organic Chemistry Inorganic Chemistry Paramekr Rcsults(rng/1) Parameter Rcsults(mg/1) (mg/kg) _ P&T:GC/MS __ Acid:B/N fa1. MTBE Radiochemistry Arsenic --Barium --Cadmium --Chloride --Chromium --__ Copper Fluoride --Iron --Lead -- --Manganese Mercury Nitrate --Selenium --Silver -- Sulfales Zinc Parameter Results (l'Ci/1) __ pH __ Gross Alpha ______ _ Cross Beta __ Conducti,i1y ______ _ TDS TOC Microbiology Paramckr Results (Col/lO0ml) B.9 Dale Rcccived ___ S_E_P~2"--"''9"9'2=-Reporlcd by _________ _ TCLP Compounds Inorganic Compounds Arsenic --Barium --Cadmium --Chromium --Lead -- --Mercury Selenium --Silver -- -- -- -- -- Rcsults(mg/1) Organic Compounds Rcsults(mg/1) V benzene 'tea CR {_/' carbon tetrachloride ----"'L"-'~-- 7:7' chlordane c...,/ chlorobcnzcnc 77' chloroform L/' o•crcsol L---" m•crcsol V p-crcsol t.,,/' crcsol 0.005 i" ~ 1,4-dichlorobenzcnc ______ _ {.,/ 1,2-dichloroclhanc 1_;_ /,./ 1,1-dichloroclhylcnc ___ c.;,,_ __ _ [./' 2,4-dinilrololucne .JL:... hcptachlor i.,,,/ hcxachlorobcnzcnc ~cxachlurohut:.idicnc ______ _ ✓ hcxachlorocthane V m CI h yl Cl h yl k Clone _.,o"._,o,.,/.cP..sLJc; __ _ _.L nitrobcnzcne .L::.._ pcnlachlorophcnol ~ pyridine V tetrachloroelhylene v trichloroelhylcne , ' J, v 2,4,5-1richloropheno\ ______ _ c/ 2,4,6-lrichlorophenol ______ _ v ,inyl chloride ....J:::::__ cndrin ~ lindanc , / mcthoxychlor ___ &~_.[oxaphcnc v·2,4:·D V2,4,5-TI' (Silvcx) ; , I. I I I I I I I I I I I I I I I I I •• N.C. Department of Environment, Jlca\lh, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Labora1ory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number _______________ _ Field Sample Numbcr ___ +"-'..2.c.....c,c...'-c;~--------- Name of Site .j'/ f-1<-,",v J;f;'7?C /4,?,<1 ,&,..,T / ID#.¢--Date Collected '?h/tz_ Collcctc<l By ~I/Krr""~ Time /.3..?o ' ' j)~ /I Site Location. __ /c&..-.«klcL.,1.0:....eO::.:t..=4"------------- Agency: £Hazardous Waste Solid Waste ---__ Supcrfuod TCLP Compounds Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium __ Ground water (1) _ Solid (5) pL,;z,4.) --Cadmium --Chromium __ Surface water (2) -.JL'Liquid (6) --Lead --__ Mercury _Soil (:1) _ Sludge (7) Selenium --Silver -- _ Other (4) _ Other (8) -- -- -- Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Resulls(mg/1) (mg/kg) Organic Compounds Results(mg/1) _LP&T:GC/MS Arsenic benzene ----V Aci<l:B/N Ext. Barium carbon tetrachloride ---- MTBE Cadmium chlordane ------Chloride chlorobcnzcnc ------Chromium chloroform ------Copper o-crcsol ------Fluoride m-crcsol ------Iron __ p-crcsol ----Lead crcsol ------ --__ Manganese --1,4-dichlorobcnzcnc --__ Mercury 1,2-Jichlorocthanc --Nitrate __ 1,1-dichlorocthylcnc --Selenium 2,4-dinit rotolucne --Silver -- -- --hcptachlor Radiochemistry Sulfates hcxachlnrobcnzcnc ----..... ·············-···---···-·-.. ·------···-··-··---·· ····--·· Zinc hcxachlorobutadicne Parameter ----Results (PCi/1) pH hcxachlorocthane ---- Gross Alpha --__ Cnn<luctivity __ methyl ethyl ketone --Gross Beta TDS nitrobcnzcne ----TOC __ pcntachlorophcnol --__ pyridine Microbiology --__ tclrachloroethylcne __ trichloroethylenc --Paramett:r Results (Col/lO0ml) __ 2,4,5-trichlorophcnol -- ----__ 2,4,6-trichlorophenol vinyl chloride ------cn<lrin --GJ> SEP 2 lin<lanc 0;1lc Rcccivt.:d rJ92 Rcp,'.rle<l_~hy --· mclhoxychlor .... :-. . : :_·:·. '.' . :·._ --.. .. ···-. --P• • . " .... -,.· ... -·.: :-.~.:.~.c-~:\~ixa·1;h~nt_:-a .... • • ·-.. .. -.. .. ... .. .. •-"•" .. . ..... ,-.. ., .... . ' ..... . ;,_,:,.· D;1lc Extr:ictcd 1/-I J .• ')!-IJJY Dale Rerorlcd . 2;4°D · ·· tJ;JI/-ff = 2,~;~:fp (Silvcx) . . ,,..... ,-, r1o ., ,... ~ Dale AnalyzcJ ()_/[ .. ,?...!.-'•< ,.'' .. I 'i-Lff-9.(l Lah Number ,..I • J ,.:. • .;j' .J ·.._ -- C:f'DWJE 13-<Y 7/.UJ •• I I I I I I I I I I I I I I I I N.~. Department of Environment, H~alth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of ~ublic Hr:alth P.O. Box 28047, 306 N. WilmingtOh Street Raleigh, North Carolina 27611 Site Number _______________ _ Field Sample Number __ ____,/:_c_l.,,,d=c>.-C..,.'---------- 'Name of Site ..1/?-M«v .fFt'z:!f/,,<747-/f'/t/T Site Location __ _,_/t"'~-'{,(,_,_r_O=i"-4.,_ _________ _ Collected By Cc..&lfcA,,;(Z#V'. ID# /4:i' l,jy Date Collcctcd ___ 4,~,~L, /~L-' /jfl'---=2.=---_;__ Time /..? f'u . 7 f)o4.;v ~ . / . / Agency: Hazardous Waste Solid Waste __ Supcrfund Sample Type Environmental Concentrate Comments _Groundwater (!) _ Solid (5) __ Surface water (2) __ Liquid (6) ____________ _ _ Soil (3) Audge (7) __________ _ _ Other (4) _ Other (8) Organic Chemistry Inorganic Chemistry Paramt'ler Results(mg/1) Parameter Results(mg/l)(mg/kg) __ P&T:GC/MS __ Acid:B/N Ex1. MTBE Radiochemistry Parameter lksults (l'Ci/1) __ Gross Alpha ______ _ Gross Beta Microbiology Parameter Results (Col/l()0ml) -- -- -- Arsenic Barium Cadmium Chloride Chromium --Copper -- Fluoride Iron Lead __ Manganese __ Mercury Nitralc Selenium -- Silver --Sulfates Zinc --_pH __ Cc,rnduclivily TDS --TOC Dale Rccciveu_s_E_P_2 __ !1_92_B_:/) Reported by ________ _ TCLP Compounds Inorganic Compounds Arsenic Barium --Cadmium Chromium --Lead __ Mercury Selenium Silver Results(mg/1) Organic Compounds Results(mg/1) [/benzene . o.r:>o3 J ~ carbon tctrar.hloride 1 , ~ chlordane i../ c.hlorobcnzcne _,0=·0=-2'-'-i .,,--- _1.c:. chloroform D,oo'-1 P, ----1.::::::: o-crcsol _fL. m-crcsol ...J..L:._ p-crcsol v crcso\ v 1,4-dichlorobcnzcnc ______ _ _LL 1,2-dichloroclhanc / , _ I/ 1,1-dichloroclhylcne ---'"-I-__ _ ~ 2,4-dinitrotolucnc v hcptachlor _.L:::hcxachlorobcnzcnc .J.L_ hexachlorohutadicne ______ _ _k hexachlorocthanc v methyl ethyl ketone ~ nitrobcnzcne v pcntachlorophcnol V pyridine .LL tc1rachloroe1hylcne _fL_ trichloroclhylcnc V 2,4,5-Lrichlorophenol {/ 2,4,6-trichlorophenol ..tL_ vinyl chloride ~ cndrin (/ lindanc ,_/ melhoxychlor ; ' V loxaphcnL:-· -_ .. _ .. _·~·: ___ ~-·~···~-··::. _;..:.c.;: ;/ 2,4-D -1L... 2,4,5-TP (Silvcx) ·-' ----- I I I I I I I I I I I I I 11 I N.C. Department of Environment, I lt:alth, & Natural Resources Soii~ Waste Management Division SAMPLE ANALYSIS KE(.!UI<.:ST State Laboratory of Public Health P.O. Box 28047, 3~ N. Wilmington Street Raieigh, North Carolina 27611 Site Number _______________ _ Field Sample Number ___ ~/,~'/~.J-o~,,Z~-------- Name of Site ,f/t:-l'fM./ .5if,V?,f/AfJA Collected By ?t&'frrug~ /4.,,&v Site Location __ tf,='i'.:w..A-"'o-"t.-'-,4,_ ____________ _ 7 l D # #11--Date Collcclcd __ ~f,c,,7 ~'---'-c/,,_fa----'---f'---'Z-"----Time_'-/_,_z-'.~/'--''5"-,----- Agency: V.:.zardous Waste Solid Waste ___ Superfund TCLP Compounds --- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- /?-Jc:u Barium --__ Groundwater (!) _ Solid (5) Cadmium -- V'Liquid (6) Chromium --__ Surface water (2) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Resulls(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) VP&T:GC/MS Arsenic benzene ~cid:B/N Ext. ----Barium carbon tetrachloride ----MTBE Cadmium chlord,mc ------Chloride chlorohcnzcnc ------Chromium chloroform ------ --__ Copper o-crcsol --Fluoride m-crcsol ------ --Iron p-crcsol ---- Lead crcsol ------ --__ Manganese --1,4-dichlorobenzcnc ----Mercury 1,2-<lichloroclhanc -- --Nilralc 1, 1-dichlorocthylcnc ----Selenium 2,4-dinil rota! ucnc ----Silver hcptachlor ----Radiochemistry Sulfates hcxachlnrobcnzcnc ----...... ·············-····-··-···-·-···------· .. ·-·-··----·····-····· Zinc hcxach lorohuta<licnc ----l'anin1cter Results (l'Ci/1) _pH hcxachlorocthane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobcnzcnc ------TOC __ pcntachlorophenol -- --__ pyridine Microbiology --__ tctrachloroethylene --__ trichlorocthylcne Pi.lrameter Results (Col/lO0rnl) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ------vinyl chloride cndrin --8,9 SEP lindanc D:1lc Received 2 --f:192 Rcporled by --mcthoxychlor .,.:_l:>atc:Ext roctcd~c<J.·1 rc.·,.-CJ;, 6'fJ..,. · --lox;.iphcnr..: --.-Da1e· Reported. . . .. . . .. 2,4-D --... ,•.···'"·.,,.· . t'J,Of/· PT -:.·.-:,;-~• ~2: .. ~ r) __ 2,-1.5-TP (Silvcx) Date Analr1.cd 9-1t,-1J... O:-'J ?-9cl Lah"Numhcr ,., ,,.., >-... , ~ ·\ \ ... C:/'1)8'JI' r!]J-} 7Uif -- I I I I I I I I I I I I I I I I I I N.C. µepartmcnt or Environment, I lcallh, & Natural Resources · Solid Waste Manageme_!lf Division SAMPLE ANALYSIS REQUt:ST State Laboratory or Public Hcallh P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number _______________ _ Field Sample Number ___ _,t.&...:./---"'c/._V:...,_Lf _____ _ 'ame of Site {/fr.HI,;,,) .,yfl'J/ Site Location 1/C-I ID# lf/r /II Date Collected 9~/f'z /..c~cYo Collected By 6,Ul£f) /44g71N/4•r?IY Time / , 7 Agency: L/Bazardous Waste Solid Waste __ Superfund TCLP Compounds -- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Commrnts Arsenic --Barium f /Otv __ Ground water (1) _ Solid (5) --Cadmium --Chromium _k'Surface water (2) Liquid (6) --Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) Other (8) -- ----Organic Chemistry Inorganic Chemistry -- P/peter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ~cid:B/N Ext. ----Barium carbon tetrachloride ---- MTBE Cadmium chlordane ------Chloride chlorobenzene -----Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ----Iron __ p-cresol ----Lead cresol ------ --__ Manganese --1,4-dichlorobcnzene --__ Mercury 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----...... -.,--. Zinc hexachlorobutadiene Paramtdcr ----Results (PCi/1) pH hexachloroethane --__ Gross Alpha Conductivity methyl ethyl ketone Gross Beta ----nitrobenzene TDS ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachloroethylene trichloroethylene ----Parameter Results (Col/!O0ml) __ 2,4,5-trichlorophenol -- --2,4,6-trichlorophenol ----vinyl chloride ------endrin -- _Bf) SEP lindanc Date Received 2 ~92 Reported by --~ethoxychlor -- l;:,;-~ ~;;;:·;cJ. iJ; 1·/~ f.~-~J ~~, · _,_ --------~~. ---~ -"' ... -.. .. .. ·c -.... "'-"--" toxaphcne _D_alc ~cp_orted 2,4-D fl;,,{/ -- f'T :; .. ',~2 ~~· -1 ~- 2,4,5-TP (Silvcx) Dale Analyzed 1-17-72-, lf-15-9 ,;;, Lab Number -- --JJ!IS 3191 (l~cvis::d 2/Yl)fJ;J} 7Uv I I I I I I_ I I I I I I 1· I I I 1.ncal i"n or Sampl:!.ng: N. C. DEPARTMENT Of HUMAN RESOURCES DIVISION OF HEALTII SERVICES SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH Chain of Custody Record Hazardous Waste Materials Genera tor __ TransporLl.'r __ Storage Facility __ Disposal Fncility Trt•,1lrnt•nl l-';il'ilil) Landfill "'/" . IC ,.,./ I . lln te Sampled __ __,o'-f~-'~''-''-· .,_7"-3-_-_ __.1.,,__,'-,'--''7_'-c.." _· _______ Time Sampled _________ _ I I I Type of Process Generating Waste -------------------------- Field Information Field Sample No. / / / "J{, //;2o3 r.h;iin ur Possession: ., 1. signature /11'?7 /1/f/J /1199 //;!,;,t./ //_;i.s,S' //,,2tJ{, title /1.:2.0o /120/ //..ZOZ 1/,20 Z I/.Zo9 gJ;_ 7/2 /7·2_ {nclusive dates inclusive dates lnstruclicms: ·complete all applicable info'rmation incl_udiiig signc1turcs, :· :···-:··::-c---•cc= •. ·,, ·:-'~-S\J brn it .. 'f i tb. ,1.M lJ.J,ts,.J"'q ~.e,s tco .. f.<J,1J11'a· , ··c. -c':':'" .. ·;_--:-... ,.;·. ~-.. nnd I I I I I I I I I I Pc. ... I ~/ ' (,c p;; lw ,4 I I ' 5 1,/ I I I I N. C. DEPARTMENT OF HUMAN RESOURCES DIVISION OF HEALTH SERVICES SOLID AND HAZARDOUS WASTE MANAGEMENT llRANCII Receipt for Samples ·The• i;.1111plt'S dl'scribed below were collected in connection with th!! administr:1t inn. ~nforcl'me11L, ~nd documentation of the: North Cnr11linn Hazardous Waste Management Rules, 1.0 NCAC IOF ( ) North Carolina Solid Waste Management Rules, 10 NCAC lOG ( Comprehensive Environmental Response, Compensation and Liability Act (CERCLA) Toxic Substances Control Act (TSCA) 15 U.S.C. §2601, ~ ~-, specifically Section 11 of TSCA, 15 U.S.C. § 2610, /ti lnspector 1 s Name Inspector's Addr l'irm Owner, Operator, or Agent Title ··--! :;AMl'LL COLLECTED SAMPLE TYPE DUPLICATE SAMPLES I SAMPLE LOCATlON NUM8[,:P. DATE TlME WATER SOIL ///ft //;',/M /SJ,,.1 {/197 ,'(l//4 L 1/,Zo /I/Yi:< ch-AL I 710• v /ll<'l'i 9/,/n: C,fLO ✓ /t 7 00 09.75 I _//_Jlo/ It: 15 v i // ,;;.,2 /0 2,c,.., I ' _Li_ ilv :J I I IU v //,;1oY' 111, LL J' o.::: ;;3,, // ~ ~1. /.J 'lo Li.~ I //,//( I/ Po") J; !5'c•o ./ _, K1•ccipt for th0 sample(s) described :IIH>VL· is hereby acknowledged: . ifk c &v:!-<c · Sign~t11rc of Inspector OTHER L,c.,,v :JLi,.,.O,f- -~L"4.(Jl( ::>luht .5< -~1,( ui-....,P J<w/,{,_/' Ul0;,1t? - OFFERED ACCEPTED REJECTED ON-SITE OFF-SITE ✓ ./ I/ i/ ✓ / i/ ✓ / v' V 1/ :/ ✓ 1/ c/ ,1 ✓ ,/ / ✓ :/ ✓ --······--·--··--v v ,/ ./ ---· ·---- Receipt/rejection samples is hereby of duplicate or split ~cknowledgcd: 7 , 7~/~ /j Signature I of Fi.i:-m O;,,;iner, Operc1tur, or Agent ,) ' /,' j _/ ·L •Tit le .. .:, . --··' STATE LAlJOMTOOY Df PUBLIC HEALTH I I I I I I I I I I I I I I I I DIVISION Of HEALlH SERVICES, N.C. DEPARTMENT Df .HUMAN RESOJRCES P.O. llOX 28047 -306 N. l<ILMINGTON, ST., RALEIGH, H.C. 27611 ORGANIC O<EMICAL NIALYS!S r· ./ p• • I ·,· "' ... '' PURG EAB l E CDM POON OS LAB NO q::i:;q :Jc, q-i-,c, ".ln '-/ .:J _-, c, =3 I q :I .;Ju '3;2. FIELD • /11Cit,, ///Ct 7 // JC/C-!. I j/QCi cet\POONO TYPE ( / ., ) ( '7) I '7 l I . -, l UNITS uo/ 1 (uo/kO: uo/1 /uo/ko) uo/1 1uo/ko-,,q/ 1 (uo/ka7 :h lorcxrethane u......-, . , u,... ,r~thane ~ ' I I dichlorodifluorcrrethane ' ' I ,invl chloride -I I :hloroethane \y' ,'/ rrethvl ene ch l ori 6e ' \."-11".1" ,:;,, trichlorofluorcrrethane ""-I I , -, ' ?thene I 1-<lichloro 0 I ..?U,ane I 1-<I ich l oro-,~ ' 'v i I I ' 1, 2-trans-di ch l oroethene " I q ,.L I I :hloroform '.:_) i i..,(_.. I I Jthane l 2-<lichloro-'0--., ! ' I eth.ane l I 1-trichloro-~ i i :arbontetrachloricSe -~-\ ' I Jrorodichlororethane )<::--,. I orrnan-e I 2-<lichloro-\ ·-! I l, 3-trans-di ch 1 oroorooene ~ I ~richloroethvlen-e '--I I chlorodibrcm:m,thane "-~ I 'V ' ""Zene ' I . .ane 1, l 2-trichloro-c-, ..... I ' I,,,__ l . 3-c is-di ch 1 Qf'YY"'lroc,er,e -\ 2-chloroethyl vinyl ether -~ ' ':>roroform \1 : I i ?thane l l 2 2-tetrachloro--i ethene tetrachloro-' ' \I '., \I to 1 uene ~""' J....,._,..,,. ,, -c7 LJ ,;4-:JC/ :h lorct:>enzene LL U--I. i -!thvl benzene "-·' . .I/ ,. ·Y I' ,,._)' ' 1cetone ·:-; '' I , ; . . ' ~-bu ta none ~ ,-' I i carbondisulfide "} ! I I :-hexanone l ' I I I t-rre thy 1-2-r _.,.n ta none , I stvrene I i vinyl acetate ·,,. ' I x y l e ""-> i+ota/ l "O \i/ HJ.., LL 1-t-1-.L.i ~..1.1.. .,... ,j LL ' / ,, r.J/,, r,v• ,,...,_.,.,,,..,',....11i..,,.-.f:-5 r.'::f:i/,,...) (j-) ( .) (. ) (.:..) I I .1 -Estimated value. -Actual value is kno,,.,,n to t>e less than value given. I Actual value· ls krrown to be greater than value given. Katerial ~as analyzed for but not 6electe<1. The nl.rrber is the Hinim.rn Detection Limit. ·NA-a Not-analyzed.---·--····'---'"-· - ./ -Ter.tative identification. '.I -On_ h'ROC .List of Priority Pollutants. I N.C. Division of Health Services JllS 3066-0 (4/86 Laboratocy) . ' o_,-,o ::i "I C; yi7· ;,, ---;J ,,..,/,o Ji;!.CJ-1 ( '7) (;ZJ uo/ 1 ..<.q/kn' uo/ 1 l'uo/ko) U-. ' - ' I ! i I ! i i ' ! ! I ' I I : ' I ' ' I ' V 7('1 I-'- I ' I I V \I ,,.533:r ,'Jr.-0 ,5cc, Ii 2.01,; 4-S , ' :-79.~ ,.77_1=, j .(, . ..- I i I I ! u ! I -4 ', i I..L-·.;j ( ..i-) (.l, I I I I I STATE LABORATORY Of f'UBLIC HEALTH DIVISION Of HEALlll SERVICES, N.C. DEPARTMENT Of .HU~ RESOORCES P.O. BCX 28047 -3()-; fi. ll!LMINGlON, ST., RALEIGH, N.C. 27611 ORGANIC °'EMICAL NIALYSIS . :::, /, .·' ':;-, ::--' .. . . ' - PURGEAB l E C0'1POJNDS LAB NO ct a ;::,c; "'" 1../.::r) o .,,,, ' Cq.., ,0~7 a·oci -;:i?'l FIELD# ,,,,,., I J,2()'", 11_,;14 , I 7"'.5 CO'IPOJND TYPE ( '7) (.:Yi ( ·7) ( I nl UNI TS uq/ I /uo/k~ uc/1 ,iQ/lio' uQ/ 1 ruq/kn un/1 ,\Jq/k~ hlorOTethane ' I ; ' u_ _ rCJT'O're thane I I dichlorodifluorOTClhane ' I I invl chloride ·,,._ I I ·h l oroethane ' I \I ,,; ' ' , rrethylene chloride \' ,:: ..., IY JQLl.. ' ' +.rich 1 orofl uoronethane ' ' Ll... I , I ' I thene 1 1--<lichloro =-...__, I ' ethane 1.1-dichloro--I 1. 2-trans-di ch loroethene "· I h 1 oroform ~ I ' thane 1.2-dichlor6-\,\ I I ethane 1 1 1-trichloro-I ! :arbontetrach l ori de -~ I i ·rorodichlorcrrethane -l ' I ! : rcoane, l 2--<lichloro--'s,. ! I : 1 3-t rans-di ch 1 oroorooen-e I C "·~ ! ' ' rich 1 oroethv 1 ene I -I . l.'.h l orodib~thane I ! ,I "\I V ..,..__ ' '.ene I ("" , -t-1,.. (lr P _ 9 :r _;i:::3 ~,,ane 1,1 2-trichloro-" i U----i...<--i.A 3-ci s-<1 i ch lo,..,....,"Jrooene ~ I I 2---chloroethyl vin·'T"l ether '✓ i I I rcrroform ~\ I I ! thane 1, 1 2 2-tetrachloro-) , ! , I ' ethene tetrachloro---,..._:, \/ v' v ·JI toluene '-) L) J " 7 114 '71 I 1177 .hlorcbenzene ["!_~!, ; , o7v, I '-i Y, ·thvlb-enzene ' --i10 ,1 :,Lj <?, '' ~' cetone --.::,.__l (....(_., -:,,7n 1--/01,, u...... -butanone ,---.', ' '7 :, " I' rix:rnd i su l fl de ~ . ! I , i I -hex a none t--I I I ! -IT€thyl-2-o'2'ntanone ,-I I I : t vrene '.J i ! ' i nvl acetate '-, J• \) I)' .,!; ,'I xvlenes i+d-ail \ 7, 1 ,o I" i.J. I ,; ·1 n.icfh -1--1-h,,J ,fe..i_J..,.,.-'' ;__,__ u_ 1, ,·,I.I, , ;_-,-.,,, ~ r.,,11 rv-1-< ~-i-cl / ;:::') 7,:;, ( _j_.] f+) 0-) I ' -Es.t1ma.led value. -Actual value is. kno,,,.,n to be less than value given. Actual value 1s. known to be greater than value given. q :< _,c;_ -1'-f ; I 1, /~ ( 7 ""/ 1 A' "'/kn' 0- I I I I i i ' i ' ./ ,; I: (..L. , ' I i r,C ~O "''7 ;)_,;J,,;:.>, I ,:,Li u.... ;r-'_ " I I , '(I I 1.'Jh u...... r+; · Katerlal was analyzed for but Ml detecte-d. The nl.JTO€'r 1s the Minirn.rn Detection Limit. -Not a·na 1 yzed. · c-' . . 1 -Tentative.identification. 1 -On NROC._Lis.t of Priority Pollutants.. J.c. Division of Health s~rvices 11S 3068--0 (4/86 Laboratory) q 1.)C/4-f! i l,~O 7 ( I., l uo/ l n.10/ka J ; J ! I i ' I I i I ' \/ 4;_, c1· Ii w ; 1'7:; IL- I I ' , v '' (-i-) I STATE LAOOAATORY OF f'UOL!C HEALlH I DIVISION OF HEALTH SERVICES, N.C. OEPAAlMENI OF .HUMN RESOORCES P.O. BOX 28047 -306 N. IIILMINGTON. Sl., RALEIGH, N.C. 21611 I I I I I I I I I I I I I I PURGEABLE CO'IPOJNOS CX\'\PCVN D chlorcrrethane brcrrorethane dichlorodifluorarethane vinvl chloride chloroethane !TE"lhvlene chloride trichlorofluorcmethane ethene 1 1-dichloro ethane 1 1-dichloro- l 2-trans-dichloroethene chlorofonn ethane l .2-dichlor6- ethane 1 1 1-trichloro- carbontetrachloride brorodi ch lorcmethane orooane 1.2-dichloro- l 3-trans-dichloroorcoene tri ch loroethvl ene chlorodibron:::roc-thane 1zene ..:~hane 1 1.2-trichloro- l . 3--c is-di ch l orooroc,,ene 2-<:hloroethyl vi nvl ether brorofonn ethane 1 1. 2 2-tetrach 1 oro-- ethene tetrach lore- toluene ch 1 orobenzene ethvlbenzene acetone 2--0utanone carbondisulflde 2-.lexanone .e.....rrethvl-2-oentanone st vrene vinvl acetate xvlene.s i+«to I) n1efh,,/--f./.,,.L,/ P/./,'t!r Ot./:J, 1' (.O~)Cld. wl-;;. OOGA/1 IC CHEM I CAL ANAL YS I 5 ?~ I) VI I U'8 NO 0-,7q4/ FIELD # 11?ne; TYPE ( ,., ) ( I ( ) UNI TS • vol I rt>o/kd uo/ I uc/kq uQ/ I uo/kn I • '- '--' : " "' ' ~l'v, i .~ ~ t-:::. i "" ~ \ 'V 'v-, \ ' 0\ -0 ¾) I -~ '-'-. __ .-.. u "' ,! .,~ I.,~ -i..L y Ji s:...J~ "" i, ,, ' '\ '7 v 1/f-; /?: (.,-) I J -Est1rr.ated value. K -Actual value is known to be less than value given. to be greater than value given. ( ) uq/l uq/kq - I -Actual value· is k:rx,,r,..n __; =_.-.)~~lerjal was analyze-<1 HA -Not"a-rialy,ed. . f ~r--;_bu l--:1!<)t de tee t.~: : --.lt-i:e ·.1"!.lP'l?Cr 1~ .. the Minirn..rn Detec~.ion Limit. l/ -Tentative identification. fl -On NROC .List of Priority Pollutants. I N.C. Division of Health Services 01!S 3068--0 (4/86 Laboraco:-v) ( ) ( I uo/ 1 uo/kq uo/1 uo/kn ·-- I STATE LABORATORY Of PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N,C. DEPARTMENT Of HUMAN RESOURCES -. , r 'IJ . fl;-.,~_=. ' • • PO BOX 28047 306 N ~ILHINGTON ST RALEIGH NC 27611 /I',, ORGANIC alEHICAL ANALYSIS f7 vi f5vJ ,>CC/NEUTRAL AND ACID LAB NO </ .J.) {7 "~ '-i '-/.~.2'1-'fO 'f,,,<../ 'I, 5 i 7,.::;,:;i. 'If)_ f -EXTRACT ABLES FIELD# 1119(,; I II C,''7 / I 11 ,!? II l'l'-1 COMPOUND TYPE ( 1~) ( ·7 ) (o<. ) (.-< ) UNITS t'PM PP/VI PPM .. ilf}/11 -N ii trosodirrethvlami ne /J JI I,<-/.( 1b1s(Z-cc.loroethvl)ether ;:-chlor"'lhenol e inol 1 _;-dic-hlorobenzene ,/ 1 4-dichlorobenzene /, a 1 :-di ch 1 orobenzene IL- b ; (2-eh loroi s=r~vl )ether hexachloroethane ~ 'litroso-di-n-nrn,..wlamine ,,:, .robenzene i snnhorone ~-:iit~heno1 2 ,-dirrethvl oheno 1 b. ; (2-eh loroethoxv)rrethane 2 4-dichloroohen~l I 1 ~ 4-trichlorobenzene ,,, c ,htha lene O. I hexachlorobutadiene (.,L. ~ -:hloro-m--cresol I ------r (ach lorocvcl (')(')pntadi"?r\€ 12 4 6-trichlorooheool 2-'Jronaphthalene ~ ~11dDhthvl ene I c. re:hyl phthalate I 2.6-dinitrotoluene I ' ~naohthene ! .l l-di'ni troohenol I lz 4-dinitrotoluene ! ' ~ "lllroohenol ' f JOrene I s-ch 1 oroohenvl phenyl ether I sJiethvl ohthalate I l -)-din it ro--o-creso 1 I ( ihenvlamine I azobenzene I l ,raroohenvlohenvlether I - t <ach 1 orob€nzene I .~entach l orooheno l I t,f"'~nanthrene I ' ~hracene ' '\j/ .;,outvl ohthalate ::?. 0 '1,,:; &;. () fluoranthene U--i,A..-i.,<.- IJ -Estimated value. K -Actual value is known to be less than value given. I -Actual value ls known to be greater than value given. l Katerial was analyzed for but not detected. The nurrber is the Hinlrrun Detection Limit. II Not analyzed, 11 --Tentative identification, ... !' -On NRDC List ·of Priority Pollutants,,, ., , C. V.i.v.u.,.i.on OIJ He,ai..th S<Vtv.i.e,e,.,, FHS 3068-0 14/86 Labof!LlJ:o~y) 1';: :- I ,_., -• /1-i-V.J •1,:J,:J_"J.3 i3 l_!.:J.293.:.L //.Zc., O I ;;,i_ o i ( 7) ( ,.2) Ff-'/Vl /'l-'/11 ,; LL.. ,1 u' I I, 0 I J, Z,_ u __ I I ' ' ,V I ;.'.<,D I iC-- I I I I ! I I I I I I I I I I \ / i Y,C> LA__. \I/ STATE LABORATORY OF PUBLIC HEALTH I I DIVISION OF HEALTH SERVICES, N.C. DEPMTHENT OF HUMAN RESOURCES P.O. BOX 28047 -306 N. \.IILHlNGTON, ST., RALEIGH, N.C. ;-)611 -'. ,~ -I .,,_,.:./NEUTRAL ANO ACID LAB NO C!.-'-~"I ,..,,q '-1.J ;)CJ 30 EXTRACT ABLES FIELD # I If 'Iv I ti cJ·7 CXlllPOUNO TYPE ( 1~ ) ( 71 PP/VI .PP/11 UNITS rene lL--iJ- ~--zidine vl henzvl ohthalate nz(a)anthracene rvsene -3 --di ch 1 orobenz id\ ne ' I ' , , (2--€thv1 hexv 1 l ohtha 1 ate n 0,0 '70.{) i-n--0<:t~l ehthalate LA_... .~ b. .zo (b lf 1 uoran thene zo(k)fluoranthene nzo (a)nvrene .!_ --'€no ( 1 • 2, 3--cd) ovrene €nzo(a.h)anthracene nzo(o h i)oervlene \ I ' I - -.. , line LL i.,C nzolc acid I iz.vl alcohol I - t:hloroaniline I tv-11zofuran ·,y _ .wl naphtha 1 ene a. z. --ethvlohenol i,,L. 1~thvl oheno 1 ~) . .5 -nitroaniline L"- ii troani 1 i ne -.1itroaniline 4 5-trichlo~henol ,1/ -, I .,----"/f:f!or"\'1.1(_ l:;<:1])5 +I-( + I (+ J - - - - - Estinute<l value. ~ • Actual value is known ! Actu.al value is kfiOWn -~ to be less than value given. to be greater than value given. '!',;/ .J ';(] I C/ ,2,)"/3.:J /;/',ii? lll'-14 (,-2 ) (.~) /1/'!'1 PP/!-1 (/(__.. ,; •/ "\)I V-V'.-- '(/ ' / -- (-) ( -) -- IL Katerial was analyzed for but not detected. The nuroer is the Hinirrun Detection Limit. NA -Not·analyzed. " -Tent.alive identification. ; -On h'ROC List' o( Pr.iori ly Pollutants . • ~.C. D.i.v,u.,.i.011 06 He_aU/i Svtv.i.c.v., r: > 3065-0 14/56 Lab01w):ofty) P4w q,2;;,c; :~, -i' c.:r:_,?;:;C/. -( i.f. /1'1/)Q //..20/ ( 71 C,:2.,\ A , ,-_;v'f r /11 f-- / L-; A \ '-lo.,) vL ·, / \ I v_. LA I I ' I \ 1· 3.0 I l.,L-I .. / 'I/ ~-.-I ,J..) ( -) '---' ,_ I STATE LABORATORY Of P\JBLI•: i!EALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES p O BOX 28D47 306 N WILMINGTON ST RALEIGH, NC 27611 ('LS00~1c aifM{iL ·ANAL·;sis P35 · p:-,J , :'"0 /NEUTRAL AND ACID II--EXTRACTABLES ■ COMPOUND N ll trosodimethvlami ne is(Z-chloroethvl)ether · _-chlorf'V"lhenol £ .·nol ~-dichlorobenzene 4--<lichlorobenzene l ·--<Jichlorobenzene I ~_.(2--<:hlorois l)ether hexachloroethane ., ~ -,ltroso-di-n..nrnnvlamine n robenzene Srv'lhorone _ 0 n i tmoheno l 2 .--<Jirrethvlohenol ,·, (2--<:h l oroethoxv)rrethane 4--<l i ch l ornnheno l l '. 4-trichlorobenzene ihtha lene exachlorobutadiene 11 :hloro--m-cresol h :achlorocvcl(")()pntadiene ~.4,6-trichlorophenol --=--)ronaohthalene ~ :naohthvlene .. :<?thvl ohthaiate 6-dinitrotoluene ~ ~naohthene ,., 1--dinitrnnhenol 4--dinitrotoluene 4 1itroohenol f JOrene --<:hloronhenvlohenvlether _<!iethvl ohthalate ~ 1--dinitro-0--cresol G.Jhenvlamine azobenzene L: wcm:iohenvlohenvlether r :achlorobenzene f:n tach l ornoheno l Q.._:nanthrene ~ .hracene d1outvl ohthalate fluoranthene FIELD# TYPE UNITS 11,ioJ... 11.~ 03 / l.2c, L/ 11-:0, ( '7) ( ,:;2..) ( ? ) ( /,; ) l'f' tVl f P/Vl .. f'f-.'/V1. r l'/11 /,I ·1,n \V I ; ' / Q. I (!,. 7 LL I ' vL J I I , IJ Estimated value. K = Actual value is known to be less than value given. L -Actual value is known to be greater than value given. I. Material was analyzed for bu\ not detected. The nuroer 1s the Minirrun Detection Limit. I~ Not analyzed. 1/ -Tentative .identification. !' -O_~ NRDC: List of Piiorlty Pollutants. /:?i-jlJl-f!?-1~~,,,,.__,() Ly.Z1·~-/.1~ZLL)?t~ II'/; C. V.i.v.u.,.i.on 06 ~HS 306&-0 (4/86 He.a.Lth Sv,,v.i.c.c.,; Laborca,tc,1,y) u...- I i i I I I , \,V (), < f'f \,\I PPM IJ. STATE LASORATOOY OF f'UBL!C HEALTH I I DIVISION OF HEALTH SERVICES, N.C. OEPAAlMENT OF H\JKAN RESOURCES P.O. BOX 28047 -306 N. li!LM!NGTOO, ST., RALEIGH, N.C. ;-/611 r. P3 vJ pci:1 OOGNHC CHEMICAL ANALYSIS f35. ('2 vJ ~c/NEUTRAL ANO ACID LAB NO 4,.2.24,'3\-9.2.2'-J·?C., Y. 2.Yi, 1 7 C/ . ..:>.2'13.? EXTRACT ABLES FIELD# I /,.J.0.-2. I ,;20 ? J /,J..o'-1 / ;.J./·,.:s CXJMPOUND TYPE ( 71 ( .,z l ( 7) ( l,~1 r'f' 1•1 f'r'/Y} p /J/t•/ ~ UNITS , / ., ene '~ L v:...... ' , , ~ :i dine .'l'l benzvl ohthalate ~ z(a)anthracene ~ vsene 3 -di ch lorobenzi dine ' ,12-€thvlhexvllnhthalate '-,--; 0 ( ti -.o -n-octvl ohthalate l.,L, V be :o(b)fluoranthenc :o(k)fluoranthenc nzo(a)ovrene J...!: · !OO ( 1, 2, 3-cd) nvrene inzo(a h)anthracene . , , nzo(o h i)oerv~ene ,,, \ J \ ·, I - 1 Ii ne /,{ (_A LL-i,L- nzoic acid : b< tvl alcohol ~ 1loroaniline , I ty--..ofuran ·,/ .c.: _ .vlnaohthalene C/. u ,_ ,thvlohenol \ I. 0 thvlohenol /, -,0 ;;i.' c) nitroa.niline i,,L. ~,(__.- -3. i troa.ni line , i troani l in€ . 4 5-trichlo=henol ' ' \ , -,/ ·, / ,,,-.,._ --~ ~ } I? R,:, '>; VJ i '.' ,4 c'''.; 7>S -t-1-I /--t-J ( -) I+ J I -) -· -- - - - - - , _ Estiruted value. K Actual value ls known to be less than value given. t Actual value ls kno,.,n to be greater than value given. 1 Katerial was analyzed for but not detected. The nmber -Not~ ,rna l yzed: . - , -TenW.llve identification. is the Minirru11 Detection Limit. 2, -Ori t-1ROC Ll.S't·o_f Priority r'o\lut.ants. I. C. v;.v~.i.;n ~6 He.a.Uh SeAv1:ce.6 Di 3068-0 (4/86 Labo1J.Q.:to11.y) 0-, C I .;. -~ 9 . .2.2';_ ?'-1 I 1.;.c, (, ( 7) /JP/-1 ' , ' / ..; 0 (,.(__, , \V l,C .. I I I I \!/ ..---,. / -,, I --- 9r_.,.,_?l_~'-;f/) //.2/>7 ( ; _, P/'A LA- \/ .36·0,0 (A__ ·,!/ LA-- I \V /, () () __ /:1, CJ c,,:___, ,I ,,-0 1-t--) ---- STATE LABORATORY Of PUBLIC HEALTH I I DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 C "",I ', .. ORGANIC CHEMICAL ANALYSIS -~kl1"1 '1-I . /NEUTRAL AND ACID LAB NO EXTRACT ABLES FIELD # //,20•1 COMPOUND TYPE (.2) ( UNITS PP/VI -, i trosodimethvlami ne ' ,( s(2-chloroethvl )ether 2 chlornohenol ino1 I :J-di ch l orobenzene _.4-dichlorobenzene 1 '.-{Jlchlorobenzene c(2-eh1orois l)ether xach lof-oethane N .i i troso--di -n-0rfV'lvl aml ne ~robenzene horone 7itroohenol -' 1-dimethvlohenol J s (2-eh loroethoxv)methane 1_ .4--dichlornnhenol 1 ~.4-trichlorot>enzene .1hthalene xachlorobutad:~ne l :h l oro -m-eres-:.; 1 I -I <achlorocvcl~ntadiene ~ ;-trichlo~henol L oronaohtha lene ' ,naphthvl ene I 111>?thvl ohthalate .6-dinitrotoluene -, ,nanhthene l--dinitr~henol 4-dinitrotolu~ne ' ,itroohenol -I '· 1orene -ehloroohenvlohenvlether ',thvl ohthalate l ;-c1; ni tro-0-creso l 1ohenvlamine zobenzene -l }N"'ITYY)hcnvlohenvlether --.(achlorobenzene ntachlor~henol i: !nanthrene ' . :hracenc \V ibutvl ohthalate _:,Z 0 , ·mranthcne [,<._ - I -Estiirated value. ~ -Actual value is known to l>e less than value given. I Actual value is kno«n I ttateria1 was analyzed , -· Not ana 1 yzed. to be greater than value given. for but not detected. The nurber I -lentative identification. ; -On NRDC List of Priority Pollutants. I . .. .C. iJ,i.v,<.J.,ion 06 He.aLth SVtv-i.c.v., HS 3068-·O 14/ 86 LaborJJ..tor..y) 1 ( ) ( l 1s the Hinirrun Detection Limit. ( l ( ) ' -- I I I BASE/NEUTRAL AND ACID EXTRACT ABLES - Irene CXJHPOJND t 1zldine lvl benzyl nhthalate nz(a)anthracene \~-vsene l-dichlorobenzidine s(2-<ethvlhexvllnhthalate 1-n-octvl phthalate 1,zo(bl fl uoranthene .1zo(kl fluoranthene nzo(alnvrene i Jeno(l 2 3-ed)nvrene >enzo(a h)anthracene nzo(o h i )n,prvlene iline nzoic acid I 'lvl alcohol :-t:loroaniline ·zofuran - : .. ,hvlnanhthalene ~vlohenol iv l oheno l 7 rii troani line . .1itroanlllne --<litroani 1 ine -, 4. 5-tri ch lorooheno l ,;.e o, 'fY 111 I.Jr'· v 5 t' .... ...._D t_,,....., -t.J. . -· -I ~ Estim:lle-<l value. I • Actua 1 va 1 ue is kno,.,,n I:. Actua 1 value is known u .. K.Jterial was analyzed NA -~ot analyzed. STATE LABORATORY Of PUBLlC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES P.O. BOX 28047 -306 N • .t!LMINGTON, ST., RALEIGH, N.C. ;-7611 ( iOj ORGANIC CHEMICAL ANALYSIS I.AB h'() /"~ J l':j(/./ FIELO # J/.:1.0'1 TYPE ( ~) ( UNITS Pf'fVI iA ' ' I /, {) [,,{___. I '\ I 1,,-L I I : I -+I -( -• I -- to be less than value given. to b-e greater than value given. for but not detected. The mrrber ) ( ) ( ) is the Minirrvn Detection Limit. ( ) ( ) .. -TenLativt: identification. :/ · , ,-/;; · l. -On NROC List of Priority Pn11utanls. !3; .. f,1/-()UC,<.A_) /..f-/4//(i,c/4._z'r)._..1 , I 'I - lj/tU'n-f1./..L /1 L),,,,J:, ,./>(!fl-1 a· . C_ V-lv-0J-tc111 {/6 Hea.lth. Ser..v,./~c.e--.:i r s 3068-0 I 4 I 86 Lu.bctJJ.-to.~yl I .. i I.· '7 I ]( • C • (u\~ DEPARPiEKT OF EN\'IROK/iENT, HEALTH, and NATURAL DIVISIOl\ OF SOLID 1-'ASTE MAl,AGEMENT Chain of Custody Record Hazardous Waste Materials ··: J..,, .1Li11n nr Sampling: Gf'nerator Storage Facility ___ Transpurll'r I I I I __ Disposal F~cility Landfill Telephone( --- 'signature ' ll;i Lt' Sampl eci __ ~\~'-/~' _--~'~/~,-+-~'-",_'-_-__________ Time Sampled __________ _ Typt' of Process Generating Waste ----------------------------1 fl~ld Information I I Fit·IJ Sample No. .', _·_ .. · ;_;__:;_ (,,.,r',' I 11 I I I Ch:lln or Possession: ~ j • ' I, . ., . 'i I 1 ,' t>:.:-·/_1_:_· ------"~·~· ._ .. ~:~.-~--~-.,~~::·~·_I_,_-._-__ ;~' ~'-I~,:,~•---- R(.'sul ts / "title ··title /°' /-' (l 1/' . -f ---ve',,.. ____ A;f,/ title / t it l e • : I 'inclusive dates inclusive dates inclus_J·,e dates I 1r1strutlinns: Co~plete all applicable information inrludinR signatures, and submit \.'i th analysis request_ f_onns, I I- I· I N.C. DEPART~,E'.\T OF E!\\'IRo::~,ElO, HEALTH, and NATURr.L RES:)l'P.CES DIVISION OF SOLID \.JASTE MANAGEMEJ,T Receipt for Samples Tl,.-•;,7;:·,1,i~"" .d_•,.s.{rihed.·bcln1., •'Pre collPcted in c·nff)rt·t•m(\;r.,;';1·;1d dorumC'nt.1t inn or the: connection with thl' .1cimini~tr:1tinn, I: <X, North Car,i!'inn Hazardous W,1stc Hanagement·Ruil'S, 15A NCAC 13A I I ) N<>rtli Carolina Sol id l.'aste Management Rules, 15A NCAC 13B Cnmpr .. hensive Environmental Response, Compensation and Li.1bilitv /let (CERCLA) Toxic Substances Control Act (TSCA) 15 U.S.C. §2601, !_l ~-• specifically Section 11 of TSCA, 15 U.S.C. @ 2610. I 0/-py' le-btc(V\ lnspector 's N.1me 4CI Finn Address 11· i rm O\.JnPr, Opc>r::itor, or Age_n_t __________ T_i_t_l_e ____________________ _ I ---------· \Ml'I.L COLLECTED SAMPLE TYPE r.1(IMK[·:P. IJATE TlME WATER SOIL OTHER ------ .!JDC]_ 3.b.!/1'. L \f"i'X) tj~...._i0' -z;--.(.,..,r-:; ± lb.r-~;, i ....Ali< 1,,),;c-(J •, 7?£1 ✓ ~it ''Ii, ,r,-,, 01 )r-, ,/ __:}Q_}_}___ . ----QJ_2_';,_ ·····--·---I -Si~A<;,c 'ru"-F' fr., v I _:1,, .~ IC>(., )_iv-_(~~~ --'/cJS ----~--···-- -I' i~ \/ _.:/_J;JJ,:_ --· -I Ii'? -----Sit.0,je -,· ~,c 'Jr ;7 '-I (1'.., 1-i -'Lei'? /Ho ··-S u,dj~ . ·7°17 H ,,; Li,· ~1,cl .. .:if J,;., C _fuz., ----V ·--·---------.. -- :OM~1 (.t!T S DUP LIC l\ TC::/SP LIT Sl\M PLES 1 SAHPLE LOCATIO:: OFFERED /ICCEPTED REJECTED ON-S !TE OH-SITE v' v -------,, v V V v V ' ---____ __J,,_• --. . ---·-------V .JL. ___;' V ,. ,/ ,/ --··· ____ v ________ .. -·-------··---··-··-· ··-----.. ·-·· "/ ,/ --~--·--------. --. V .. ,, V __ _v' .... --... . .. . .. ... -. ... ---····-· Receipt/rejection of uuplicate or split snmples is hereby acknowledF,ed: /J . A' . / )': ~/<'.' -.. -J ...::-::-:/-·r7 t'_.; - Signatur;, of Finn 01..ncr, Operatur, or Afent ) -,J .,,.... ~ Title --·-----------,J ... ,R _:,_,,I ( )/H', I ------··--------------------------------------- ,1 .,I .", I( 1,· ",1.,,,,, ~ 1_-;1 ,. I I I I I I I I I I I I I I I I I I ------------------------------------------------- N.C. Department of Environment, l lcalth, & Natural Rcsoun::es Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 ·le Number ----------------Field Sample Number ___ q,__,0=0'--''SJ"------------ Name of Site S,U{'y1YI M.p-/-,'e, /&AA: fu/,eq,n'>LJ Site Location Cu{trf o.___ Collected By (1 /e,_ser-/Mart,n / Ooo-r" ID# ('3/i-1/21 I I I ' Date Collected /3 /) i /9 "J. I Time /&;J...o ----'-"=""---- Agency: _'/._Hazardous Waste Solid Waste __ Superfund TCLP Compounds -- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments 1_ Arsenic L.o_cj ___:L_Barium ..:,, ~0 __ Ground water (1) _ Solid (5) 1)0-S X. Cadmium L..o ,.-..18 )( Chromium Le:, lO __ Surface water (2) _ Liquid (6) 'I--Lead L.o -SD --___IS_ Mercury ..:::.. Q -c:, :;)__ _ Soil (3) __i_ Sludge (7) __L__ Selenium L.... 0-0~ -1::_ Silver «:(a_ lo Other (4) _ Other (8) -- ---- Organic Chemistry Inorganic Chemistry -- P'1rametcr Resulls(mg/1) Parameter Resulls~)(mg/1.g) Organic Compounds Results(mg/li P&T:GC/MS _£_ Arsenic L.. ._-\_ 8, benzene = Acid:B/N Ext. -- X. Barium :':Lo carbon tetrachloride -- MTBE _L_ Cadmium .L._ \ l& chlordane ---- Chloride chlorobenzene ------ --_L Chromium L.:;),o chloroform -- --__ Copper o-cresol -- Fluoride m-cresol ------ --Iron __ p-cresol -- --...:L. u:ad ') I cresol -- --__ Manganese --1,4-dichlorobenzene --_L_ Mercury c:-,.15 __ 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --" Selenium ""--'). 8 2,4-dinit rotoluene -- ___:;,::_ Silver L.. ,;,__o __ heptachlor Radiochemistry Sulfates hexachlorobenzene ---- ...... _. Zinc hexachlorobutadiene ---- Pardmeter Resulls (PCi/1) pH hexachloroethane -- __ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzcne ------ TOC __ pentachlorophenol -- --__ pyridine --Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride cndrin --lindane Date Received Reportc_q by. __ methoxychlor ·-· . --toxaphene Date Extractcu Date Reported 2,4-0 -- --2,4,5-TP (Silvex) D;11c Analyn.:d Lab Number -- I I I I ------------------------------------ SAMPLE ANALYSIS REQUEST Stale Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Strcc! I I I I I I I I I I I I I I I I I I N.C. Department of Environment, I lc~llh, & Natural Resources Solid Waste: Management Division Sile Number ---------------- Raleigh, North Carolina 27611 Name of Sile <;t~o,,1 >Rfi•'-/AA{'r tfM\j'•'<.u Site Location. _ _,:C"'u'"W-"-'"'C-"'---------------- Col!ected B y§/o7,, ( lnwh V\ / lli(rt /skpki<JD # ~b1 I I '.6 I, Dale Collected __ 1,-,/c_:1c,(_'t._;z,:._ ____ Time () '73 5 ' ' Agency: I. Hazardous Waste Solid Waste __ Superfund TCLP Compounds Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments ____x__ Arsenic .L_ o_ o '-\- "-Barium o. '--J 9 __ Ground water (1) _ Solid (5) -P5_-S ___L_ Cadmium 4-Q 06 ___L Chromium L,=,-,o __ Surface water (2) _ Liquid (6) _L Lead L_o.so _L Mercury .c:::_0-C,h. Soil (3) ___K__ Sludge (7) __x__ Selenium .c._ o _ o:J __k_:_ Si Iver .L_o. ,o _ Othe.r (4) _ Other (8) -- -- -- Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) · Parameter Results~(mg/kg) Organic Compounds Results (mg/I) _P&T:GC/MS ___L_ Arsenic L_'\_e, benzene -- _ Acid:B/N Ext. __Y._ Barium 100 carbon tetrachloride -- MTBE __i5'._ Cadmium L. \ LP chlordane ---- Chloride chlorobenzene ---- --__z__ Chromium :;,_ \ chloroform -- --__ Copper o-cresol -- Fluoride rn-cresol ------ --Iron __ p-cresol --__L Lead ' -\ cresol -- ----Manganese 1,4-dichlorobenzene -- --__L Mercury Q -i~ 1,2-diehloroethane --Nitrate 1, 1-dichloroethylene __,y;_ Selenium L..7 8 --2,4-dinitrotoluene _!i__Silver .L__ ::i._ 0 __ heptachlor Radiochemistry Sulfates hexachlorobenzene ---- ······-·· Zinc hexachlorobutadiene ---- Parameter Results (PCi/1) pH hexachloroethane __ Gross Alpha --Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ----TOC __ p_entachlorophenol -- --__ pyridine --Microbiology --__ letrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindanc -- . Date Rccciycd Reported by . __ . _ "]elhoxychlor ·---toxaphene D"lc Exlr"clcu Dale Reported 2,4-D __ 2,4,5-TP (Si1vex) Dote Anulyzcd Lab Number ---- I I I I I I I I I I I I I I I I I I I ---------------·------·-·----------------- :S:.C. Department or Environment, I lea Ith, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory or Public i"lealth r.o. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number -----------------Field Sample Number ___ .,,_,=----'------------ . Name of Sile Srgrrtm ~1½/4M e:rte{pcc'&d Site Localion _ __.E;""-"'u.LJfo-L . .,,{e,_""-------------- Co llected By {j lo. ,;e~/i-.. 0_,.f,·11 ,/,);,or .,.._ ID# 1:J,b<l/11 Date Collected _ ____;'lJ./--'1--1/'-Cf-'-"2,'-----Time.. /(,, 20 ~-'------------------, Agency: ....x__Hazardous Waste Solid Waste __ Superfund Sample Type Environmental Concentrate Comments _Groundwater (1) __ Solid (5) Surface water (2) Liquid (6) ___________ _ Soil (3) _L__ Sludge (7) _________ _ _ Other (4) _ Other (8) ___________ _ Organic Chemistry Inorganic Chemistry Parameter _ P&T:GC/MS _ Acid:B/N Ext. Results(mg/1) Parameter _I::'._ Arsenic LBarium _iL. Cadmium Resullsp,} (mg/kg) "'-' .. R MTBE Chloride v Chromium __ Copper Fluoride Iron ~Lead __ Manganese .....u_ Mercury Nitrate ...JL Selenium !----------------, _:,L Silver Radiochemistry .......... --------------l Pa rd meter __ Gross Alpha Gross Beta Results (PCi/1) .... Microbiology Parameter Results (Col/IOOml) Sulfates Zinc --pH = Conductivity TDS --TOC ------.. 51 Date Received Reported hy --~.------------------- D;itc Extr:icic<l Date Reported ------------------ D;itc Analyzed _________ Lab Number TCLP Com;.,ounds Inorganic Compounds Results(mg/1) v Arsenic L. o . a c\ ✓ Barium O -3 8 ✓ Cadmium L O _ o8 -'<'.'... Chromium L. o, 1 0 _LL Lead L. = .. 50 v Mercury .L..o .. o ~ v Selenium ..L. o . c j i/ Silver Lo_ ,o _______ .. _________ _ ------------------ Organic Compounds benzene --carbon tetrachloride Results(mg/1) ---------cHordane chlorobenzene --chloroform o-cresol --m-cresol p-cresol --cresol ----i,4-dichlorobenzeoe ______ _ 1,2-dichloroethane . --1,1-dichloroethyleoe 2,4-dinitrotoluene = heptachlor hexachlorobenzene hexachlorobutadiene ------- ----------he.xachloroethane ----methyl ethyl ketone ______ _ nitrobenzcne pentachlorophenol = pyridi~c __ tetrachloroethylene trichloroethyleoe --2,4,5-trichloropheool = 2,4,6-trichlorophenol ------- --vinyl chloride eridrin --lindanc __ methoxychlor __ toxaphcne 2,4-D = 2,4,5-TP (Silvex) I I I I I I I I I I I I I I I I I N.C. Department of Environment, · I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory:>( !"ublic Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number -------------Field Sample Number __ f.~D~-~{_..(,,"" ___________ _ Name of Site r)(@-,.,,.M {g_p/-;-c_ /4!1A -l Collected ByG-/,;se, Mo.t'k"-(Do,,·~ , ' Site Location_~£=u~b=6=c;_~-------------- ID# -,,;\Ii I Date Collected_--'~'..f./--'1--+/'-'f,.__Z-=------Time_~//~/_'$~-- Agency: II' Hazardous W asle Solid Waste __ Superfund TCLF Compounds ----- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments J Arsenic -"--o. co'-j ✓ Barium Cl.·::, d- [3-5 --Cadmium .:'...a. aR __ Ground water (1) Solid (5) ✓ ✓ Chromium .'....~ .IQ __ Surface water (2) _ Liquid (6) _jL_ Lead -<:..o • .50 v' Mercury -<'....o.c~ _ Soil (3) ~ Sludge (7) ✓ Selenium -<:..a.a'--\ 7 Silver L_g .. \Q -- _ Other (4) Other (8) ------ Organic Chemistry Inorganic Chemistry -- P~·:ameter Resulls(mg/1) Parameter Results ~mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS v Arsenic L...""\.'?, benzene ---- __ Acid:B/N Ext. ✓ Barium )\0 carbon tetrachloride -- MTBE __\L. Cadmium -"----\ l.a chlordane ---- Chloride chlorobenzene ----·- --L Chromium C, \ chloroform -- --__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol -- ....!L Lead "~ cresol ---- --__ Manganese --1,4-dichlorobenzeue --..JL Mercury Q,elS __ 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene \/ Selenium L7_s5 2,4-dinitrotoluene v Silver L,..:,.,o --heptachlor --Radiochemistry Sulfates bex;,chlorobenzene ---- ······-·· Zinc hexachlorobutadiene ---- Pan1mett:r Results (PCi/1) pH hex;,chloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ----TOC __ pentachlorophenol -- --__ pyridine ._ Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vir,yl chloride eridrin --lindane -- Date Received Rcporte_d by __ methoxychlcr -~ tox"iiphene Dote Extracted Date Reported 2,4-D ---I V _ 2,4,5 TP ,Sil ex) Dote Analyzed Lab Number -,---c-=,-~--------------- 1) f IS 31'JI {Rcvi:-cd 2/9Jj i I I ' , I I I I I I I I I I I I I I I I I I I N.C. Dcpanmcnt of Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number Field Sample Number __ __,q-"D::..· ,_/ ,._g,_ _________ _ ----------------- .Name of Sile )f;W:IJ vpkv /AM 0-Wprr¼ Site Location. _ _,.e;:"'"'"""k,,:,.._ ___________ _ Collected By(j/w, lt1wli'n lvcccn.. ID# n/411-Date Collected __ ._9..:,,1--/1'-l-/-~.,_,Z.,=._ ___ Time J3.ifo ' I Agency: _I._ Hazardous Waste Solid Waste __ Superfund TCLP Compounds --- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments v Arsenic L_ 0-Cl~ ✓ Barium Q.3:± __ Groundwater (1) Solid (5) va-s v' Cadmium Lo .oB v' Chromium Lo 11: IQ __ Surface water (2) _ Liquid (6) V Lead L.. o. 50 --~ Mercury ""--o .o;;,... _ Soil (3) __x_ Sludge (7) V Selenium L.c,_ 0 '.::l _!c'._Silver 4Q-l0 _ Other (4) Other (8) -- .. ---- Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (!lli"')(mr ·'Iv 0,-;;anic Compounds Results(mg/1) --P&T:GC/MS ,I Arsenic L_ :J . 'el benzene --__ Acid:B/N Ext. -✓-. Barium Bo carbon tetrachloride --MTBE _le'.'._ Cadmium L... \ \.Q chlordane ----Chloride chlorobenzene ------ --v Chromium "-\ '3 chloroform -- --__ Copper o-cresol --Fluoride m-cresol ---- --Iron __ p-cresol --_.,L'.Lead ~--cresol ---- --__ Manganese 1,4-dichlorobenzene -- --_.!::__Mercury 0. d,:l --1,2-dichloroethane ----Nitrate __ 1,1-dichloroethylene v Selenium L.,_-2, 2,4-dinitrotoluene ,/ Silver ..:. .:,.._Q __ · heptachlor Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene Pan1m~t~r ----Results (PCi/1) --pH hexachloroethane __ Gross Alpha __ Conductivity __ methyl ethyi ketone Gross Beta TDS nitrobenzene ----TOC __ pentachlorophcnol -- --__ pyridine --Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol --__ vinyl chloride --endrin --lindane Date Received Rcpuncd by __ methoxychlor toxaphene -- D"tc Exlr"ctcJ Date Reoorted 2,4-D --2,4,5-TP (Silvex) --Dale Analyzed Lab N1Jmbcr -- I N.C. Department o( Envil_'Onment, SAMPLE ANALYSIS REQUEST . . · I lcallh, & Natural Resources 1 · :: :" Soi.id W"a.ste M8nagelllerlt Division State Laboratory or Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 I I I I I I I I I I I I I I I · Site Number ----------------Field Sample Numbcr __ q._0"--='0_7.,_ __________ _ Name of Site S','1M01 fie_p/-fe, ,1/±fM: {nterpri¼ Site Location Zll We Collected By {i/a.g I" /-.1c,_.-I,.._ ID# /3 /,f J Date Collected R /:JI / C/ Z,, ' Time /'5 30 ---'-'="'----- Agency: ~Hazardous Waste Solid Waste __ Superfund TCLP Compounds -- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium Pt-1u --Cadmium __ Ground water (1) Solid (5) --Chromium -- Surface water (2) _x_ Liquid (6) Lead ----Mercury _Soil (3) _ Sludge (7) Selenium --Silver -- Other (4) _ Other (8) ---- -- Organic Chemistry Inorganic Chemistry -- Parameter Resu Its (mg/I) Parameter Results~)(mg/kg) Organic Compounds Results(mg/1) --P&T:GC/MS _'L_ Arsenic "---\5 benzene -- Acid:B/N Ext. ...1.._Barium "'--I :::i carbon tetrachloride ---- MTBE ...:L. Cadm'ium .L_ ~ I chlordane ---- Chloride chlorobenzene ---- --....L Chromium .L... oB chloroform -- --_·_ Copper o-cresol --Fluoride m-cresol ----= p-cresol --Iron -- --...:t_Lead L.. ,;,6 cresol -- --__ Manganese 1,4-dichlorobenzene -- --__x__ Mercury L..s;,.c""i 1,2-dichloroethane --Nitrate = 1,1-dichloroethylene _L.. Selenium L._ \ 5 2,4-dinitrotoluene ...L Silver .L.. ?:,8 __ heptachlor Radiochemistry Sulfates hexachlorobenzene ---- ······-·· Zinc hexachlorobutadiene ---- Par.tmetcr Results (PCi/1) _pH hexachloroethane -- __ Gross Alpha --Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ----= pentachlorophenol TOC -- --__ pyridine --Microbiology ----tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----__ vinyl chloride eridrin --lindane -- Date Rccci•1cd _ Reported by __ methoxychlor __ toxaphene Dale Extraclcu Dale Reported --2,4'.D --2,4,5-TP (Silvex) Da!c Analy,cd Lab Number --... ... . -..... - - I I I I I I I I I I I I I I I I I I I N.C. Dcpartmc:-:( or Environment, l lcalth, & Natural Resources Solid Waste Managcmcr:it Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O."Box 28047, J06 N. Wilmington Slrcct Raleigh, North C.arolina 27611 •· Site Number _______________ _ Field Sample Number ___ °I""'--'-<'------------ Site Location_-=~=="'---------------- Collected By Glc,w fttadu, /r.w,r1,,_ ; I Date Collected tj /, (jv I Time_j!:il_:::;_ __ _ Agency. ¥.. Hazardous Waste --Solid Waste __ Superfund TCLP Compounds Sample Type inorganic Compounds Results (mg/I) Environmental Concentrate Comments Arsenic --Barium '°DI -I, I --__ Ground water (1) _ Solid (5) Cadmium --Chromium --__ Surface water (2) _lL Liquid (6) Lead --__ Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- ----Organic Chemistry Inorganic Chemistry -- Parameter ll.esults(mg/1) Parameter Result.s~(mg/kg) Organic Compounds Result.s(mg/1• _P&T:GC/MS v Arsenic L_\ s benzene ----__ Acid:B/N Ext. V Barium .L.)'::, carbon tetrachloride --MTBE V Cadmium L. 3) chlordane ------Chloride chlorobenzene ----_iL Chromium L. 3 '?, chloroform ----__ Copper o-cresol ----Fluoride m-cresol ---Iron p-cresol ------_k'.'.Lead L. .3 :;a, cresol ----__ Manganese --1,4-dichlorobenzene --~ Mercury -"--0-03 __ 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene V Selenium L. I !::> 2,4-dinitrotoluene v Silver L. ?,,::>, __ heptachlor Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene Pardmt!ttr ----Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobcnzene ------ --TOC __ pentachlorophenol --__ pyridine Microbiology --__ tetrachloroethylene -· __ trichloroethylene --Parumett:r Results (Col/lOOml) __ 2,4,5-trichlorophenol ----2,4,6-trichlorophenol --vinyl chloride --cndrin --lindane Date Rccciv::.C ---Reported by methoxychlor -- --toxaphene Dale Exlraclcu Date Reported 2,4-0 --__ 2,4,5-TP (Silvex) O;.itc Amilyzcd Lab Number : I,,,..,:.-' ' DI !S JI) 1 J,_ .. ~cd .. Ul'I -- I i I ! I I ' i I I I I I I I I I I I REFERENCE 22 I I I I I I I 11 I I I I I I I I I I I I I I I I I I I · Ref. 22 State of North Carolina Department of Environment, Health, and Natural Resources 512 ~,orth Salisbury Srreet • Raleigh, North Carolina 27604 Division of Solid Waste Management James B. Hunt, Jr., Governor T,iephon< 919-733-2178 Jonathan 8. Howes, Secretary February 11, 1993 MEMORANDUM TO: THROUGH: FROM: RE: Dexter Matthews, Chief Solid Waste Section Jerry Rhodes, Chief// Hazardous Waste Jrection Doug Holyfield1n.iead Waste Management Branch Sigmon Septic Tank Service -AAA Enterprises Eufola (Statesville) I have enclosed for your review a copy of our case development sampling investigation of the noted site. With Mr. Sigmon's failure to comply with our request to sample the septage impoundments, we initiated our own sampling investigation. This investigation included sampling water, liquid, and sludge samples from eight (8) septage pits and three water samples from off-site residential wells. According to Mr. Sigmon, the septage pits have not been utilized since the spring of 1992. Our sampling results indicate the presence of various hazardous constituents, primarily phthalates and phenols, however, no constituent exceeded TCLP levels to indicate a characteristic hazardous waste and we have no information to substantiate the disposal of listed hazardous wastes. Therefore, we cannot establish RCRA land units which would require implementation of closure/post-closure plans or ground water assessment/remediation. As such, our attorneys have advised us that an enforcement action would be very difficult to prove, especially with the site being non-operational. Subsequently, with regards to the septage units, we respectfully refer this site to you for evaluation under your program. In conclusion, by copy of this transmittal, we are notifying the Division of Environmental Management of our results of the off-site residential well sampling which exceeded their 2L Standards. The Munford well (lt9032) contained 0.09 mg/1 manganese, 0.007 mg/1 PO Bm )7687, R..1ki[.:+,, North Carolina )76\1•7687 Tclcphom: 919-733-49R4 LD., 9\9-733-051) I,., ~::'.\ I ,_,, ll 1/ I I I I I I I I I I ·I I I I Page 2. mercury, and 23.35 mg/1 nitrate. The Davidson well (#9033), no longer in use, contained 4.43 mg/1 iron, and 0.83 mg/1 manganese. Please contact me or Bob Glaser of our Groundwater Unit should you have any questions regarding the investigation. Also, Keith Masters and his staff is available for any support in the field. Attachment: cc: Mike Kelly Keith Masters Bob Glaser Judy Bullock Chris DeRoller -DEM Mooresville I I I I I __ I I I I I I I I •• I-· I TO: FROM: RE: December 30, 1992 M E M O R A N D U M Keith Masters Laurie Martin Site investigation at Sigmon Septic/AAA Enterprises in Eufola. On August 31 and September 1, 1992, Bob Glaser, Pete Doorn, Gray Stephens and Laurie Martin of the Ground Water Unit collected water, liquid and sludge samples from eight septage pits at Sigmon Septic and three water samples from nearby residential wells. Sigmon Septic/AAA Enterprises is located on Eufola Rd. (SR 1333) in Eufola'(near Statesville). Lafayette Atkinson, Safety Officer, was also present during the sampling. Eight active septage impoundments were located near the rear of the property. According to Barry Sigmon, no septage had been added to the impoundments since Spring 1992. Two additional ponds, reportedly closed for six or seven years, were also on site. A dirt road, accessed from Buffalo Shoals Rd. (SR 1004), runs behind the property. Several residences with private wells are located along this dirt road. Water samples were collected from the wells located on the Morgan, Munford, and Davidson residences (see attached sketch). Field sample numbers 9031 (inorganic) and 11220 (organic) were collected from the Morgan well. Field sample numbers 9032 (inorganic) and 11221 (organic) were collected from the Munford well. Field sample numbers 9033 (inorganic) and 11222 (organic) were collected from the Davidson well. The analytical results for these samples are attached. The sample collected from the Munford well (#9032) contained 0.09 mg/1 manganese, 0.007 mg/1 mercury, and 23.35 mg/1 nitrate. The sample from the Davidson well (#9033) contained 4.43 mg/1 iron, and 0.83 mg/1 manganese. (According to Davidson, this well is no longer used for drinking water.) These concentrations exceed the North Carolina water quality standards for ground water (Tl5: 02L I_ I I I I I I I I I I I I I I .0200). Liquid, sludge and/or water samples were taken from each of the ''active'' ponds (see attached sketch). Field sample numbers 9007 and 9008 (inorganic), and 11196 and 11197 (organic) were collected from pond #6. Field sample numbers 9009 (inorganic) and 11198 (organic) were collected from pond #7. Field sample numbers 9010 and 9011 (inorganic), and 11199 and 11200 (organic) were collected from pond #5. Field sample numbers 9013 and 9014 (inorganic), and 11201 and 11202 (organic) were collected from pond #4. Field sample numbers 9015 and 9016 (inorganic), and 11203 and 11204 (organic) were collected from pond #3. Field sample numbers 9017 and 9018 (inorganic), and 11205 and 11206 (organic) were collected from pond #2. Field sample numbers 9019 (inorganic) and 11207 (organic) were collected from pond #1. Field sample numbers 9020 (inorganic), and 11209 (organic) were collected from pond #10. The analytical results for these samples are attached. Sludges The contaminant concentrations found in the sludges taken from the ponds were below the TC levels. The totals analyses for the organic constituents in the sludges (#11197, #11200, #11202, #11204, #11206) indicated concentrations ranging from not detected (ND) to 90,000 ppb bis (2-ethylhexyl) phthalate, 25,000 ppb 4-methylphenol, 16,533 ppb toluene, 9000 ppb 2- methylnaphthalene, 8000 ppb dibutyl phthalate, 7000 ppb 1,4 dichlorobenzene, 4000 ppb naphthalene, 2500 ppb chlorobenzene, 1155 ppb xylene, 1000 ppb 2-methylphenol, 624 ppb acetone, 288 ppb ethylbenzene, 200 ppb 1,2 dichlorobenzene, 156 ppb methylene chloride, 100 ppb 1;3 dichlorobenzene, 70 ppb benzene, and 18 ppb carbondisulfide. The totals analyses for the inorganic constituents in the sludges (#9008, #9011, #9014, #9016, #9018) indicated concentrations ranging from ND to 200 ppm lead, 110 ppm barium, 51 ppm chromium, and 0.29 ppm mercury. Liquid {excluding water) The contaminant concentrations found in the liquids taken from the ponds were below the TC levels. The totals analyses for the organic constituents in the liquids (#11196, #11205, #11207) indicated concentrations ranging from ND to 360,000 ppb bis(2- ethylhexyl) phthalate, 11,000 ppb dibutyl phthalate, 7000 ppb phenol, 6000 ppb 4-methylphenol, 1277 ppb toluene, 1273 ppb acetone, 1000 ppb 2-methylnaphthalene, 148 ppb chlorobenzene, 51 ppb xylene, and 33 ppb benzene. The totals analyses for the inorganic constituents in the liquids (#9007, #9017, #9019) indicated concentrations ranging from ND to 2.3 ppm lead, 0.19 ppm chromium, 0.021 ppm cadmium. I I I __ I I I . I I I I I I I I I I I I Pond Water The totals analyses for the organic constituents in the pond water (#11198, #11199, #11201, #11203, #11209) indicated concentrations ranging from ND to 6000 ppb dibutyl phthalate, 1000 ppb bis (2-ethylhexyl) phthalate, 735 ppb 2-butanone, 392 ppb acetone, 208 ppb toluene, 19 ppb methylene chloride, 14 ppb chlorobenzene, 10 ppb xylene, 6 ppb benzene. The totals analyses for the inorganic constituents in the pond water (#9009, #9010, #9013, #9015, #9020) indicated concentrations ranging from ND to 3.58 ppm barium, 2.69 ppm lead, 0.25 ppm chromium, and 0.131 ppm cadmium . I'. I ' ' I , .,. ---_/ -·· . 7 •. ~ I 1_: ~-~ ,.....,.. I. D I . • □® I R.,.,,1..-,) -r,-,11( -- - - - --- - -----~~ ---}-- -----1-----1 ---------I----- P7· w IS +-·----1-------____ , ___ _ 1'•,-,0_"_1 I . --1 .for.-.t:...-__ : ~J\tl '2 · _[,,,(l,U'•'.------ ?c,,,,I 'l I I I I I I I I I I REFERENCE 23 I I I I ii II I I I --· - -lJAO NU. Ll 7_ · _!Q SEAi AL NO. - - - - -LitJparlmsrn of E:nv1ronm011l, Heall -, --llllltllll .. ~-• o .. v~ •-- DATE RECEIVEo,)_ Q ,___d TlmeCl r:) -" LONG. ,\o 5S O.s·" md Natural Hesources r: lt ) • 2 . 6 , re; Division of Environm011lal ManaJomonl L£; . ~~-l --'-~ oport lo: AnO, FRO,~ flRO, WaRO, WiRO, Ct~AJWa~,!jt;O~lFULJY ~~~~: by ~ r,om Uu~ SAMPLE r 0 F1IOR[['( O· DA r A EHJHY BY: 7// CK: bJ?!-~ .Sf\O, KiflSIOll ro 0 lhor llppod by: Ous.~·ur.io.~ 01t1or (Z] ROUTINE EMERGENCY DATE REPORTED: (,h,D//.J --------------- JLLECTOR(SJ: Ou;,,/1,r /;p,;/kclDATE ELD ANALYSES 5?5/73 Ow nor TIME /,F,7'0-/o':f~/PURPOSE: BASELINE, COMPLAltiT, {cl rel e COMPLIANCE, LUST, OTHER on•J · Poli. ~;c1/::: S IE :C(.JI Yi' ) 7,0 S C .-;,:;(, BI "°""C kU( i{ ----------------400 pee. and. B ◄ _,-J <-:i-~ Localion or slle Odor -~a_,.,_a.,9,eYu_tL''"''~~c~r, ... r11y Doscrlplion al sarnplino point · J /u/-·,1 poo,unco O,i.;y /irrdoiC l aslo __ .._ __ ,. ___ _ _1 / 1 Sampli1lQ Molhod ,S kc I (pump. bollor, etcJ _").-.-,:-,/, Sa mp I e In tor v a I _ __,-c.,<_'-'~---~3"'-'"'"'------- l Id An a I y s i s By: ~IM=,:;>-u/60.'_,e.,_,_( _____ _ Remarks ,IJOflATOllY ANALYSl'S OOUi, '" -coo tt1on '" -coo lo• '" -, Colllo1m:1.U f • C •l Jl616~/Q0 ' Collfo,m;l-lf 1 01• I JI !,O 4 !QC '" - Tu1bldll1 " - - OH "' - All 1!1nlly lo '" u <JO - Alk•llnl1y ro "' .., "6 - C1rborut, .. 6 - Dlc ■1bon11o "" - A_runlc:10111 I 00 2 C ■rbon dloddt .. , Chlnrlde "" - Ch1nml...,n:tl1, \Oll Colot:lu. .. '" C: 1 • nl <1• "" J Com11H1nl1: 1/-5-1 fllcV. IIJ90 moll )( moll ,ng/1 I 1oom·1 1100ml rng/1 H!U unl11 mofl mg/I mo/I m Q II ';{ """ mall y .. ,1,1,1 UD JI Pl·Co --- moll -+"~/_,~,~' ,~, ... r::~,~--r~"~-~·· ~-... f~j'.;~-~S~~=-_ r ._(,, ,· , Ao· ..-r (2 ~. I (pumplno limo. air lernp, alc:- ,,;,,.,cf ,l1 C /...c I\ e'>,.. ( 1 "C 1,.-.-p c ....,, ,· µ I ..--0 ,.f Olu. SolJd1 10)00 <-/-,;i D moll Ao· 511vu 1011 uo/1 0,1,,1nochlo,ln• f'a1ll11lda1 fluoride '" mg/I Al • Aluminum I IO& UQ/i 0, o • nop r, o 1phor u 1 f'11ll0Jda1 ll■1dn1u:To111 000 moll ;x o, · Uallum "\001 '-\ I 0 ""/I tla,<ln■u (non·cub) "' mg/I c, Calcium ". moll Ac Id tt11dl11lda1 -· Ph1nol1 ::121JO •>OIi Cd Cadmium 1 o 2 r UQ/1 Sp■clllc Cond. " ul.tho1/cm 7 Ch1om!um:Toi1I IOJ ◄ uo" B••• I H I ull &I [1lr1t:llbl1 Orgu1l•1 Sulf■ I• '" molt Cu • C.oppa1 1041 U0 fl Acid £1!r1c11t>l1 Q1g1 rel 111 Sullld• l<S mg/I f. iron IO 4 ~ ug II 'X Ho Uucur, , 11100-< c-1. /J ug II x· Pu1g11t>l1 Oro1nlc1 (VOA ti o Ill I J K f'o1111ium "' mg/I "' · U1on11lum 1117 mo}r l, 2 Olbromo1ll'llnl 1£08) "". '-"•nu•n••• 10Hi, UQ II , .. Sodium '" molt Ntl3 "N 6l0 0, 7J-mg/I "' IH c ~ • 1 I 06 I uo/1 ~~JE~. c,·:;-r·, lKH .. H 62 5-mg/J HOJ ,. HOJ "H 630 7,3 moll 4 <'b · l • •d IO~ I '1 c-.._; UQ/1 s, S•l•11lum 1141 UQ /I Or.1t,1 ;·_.:-·_-_:• '~~J.•1.-:7 .; .i •• ~,:, .'-";;-.,.1!.'L . ;-•-<;:, ,,,_ f>;l ol■l 11 P 66$ moll ]o Zinc \091 . ug /I Jl fl i ·, --''.')j DIYIS . . /," 'lr ~ Ii' :1r-:ni11 Ir (t'ln•UiT:1 " !,•: ,, 11£u11,ij1' .... , •Al DFI/C[ For Dlsso/vad Analysis -submit llllerod sample and wrile ·01°· '1 block WJd!n Coov -Grnu,,clw;:tlnr Cnn!r;tl OfHr_.0 Ynll,1w r.oov -I ,n,tl Ofllco rink Cnnv. (';()ntr:11 Fl~• f1nlr'kinrnd f'.nnv. I nl, . I I LAB HO, JG 701 I eEPORTBD BY . _7:!'-',-""7"'-- -CHECKED BY uk~ • RBViEliED BY @-.- • I SAMPLE TYPE: WATER I CASI VOA TARGET COMPOUND I 75-35-4 1,1-Dichloroethene 0. 75 75-09-2 Methylene Chloride 0 .25 156-60-5 trans-1,2-Dichloroethene 0, 7 5 75-31·3 1,I·Dichloroethane 0, 2 5 I 590-20-7 2,2-Dichloropropane 0 .25 156-59-\ cis-1,2-Dichloroethene 0. 2 5 67-66-J Chloroform 0.25 I 74-97-5 Broaochloroaetbane 0, 7 5 71-55-6 1,1,l·Trichloroethane 0.25 563-58-6 1,1-Dichloropropene 0. 2 5 I 56-23-5 Carbon Tetrachloride 0.75 107-06-1 1,1-Dichloroethane 0,15 19-01·6 Trichloroethene 0, 15 I 78-87-5 1,1-Dichloropropane 0,15 75-11-4 Bro;odichloronethane 0.25 H-95-3 Dibronoae•.nane 1 .0061-01-5 cis-1,3-Dichloropropene 0,25 I 10061-02·6 trans·l,3-Dichloropropene 0. 25 19-00-5 1,1,1-Trichloroethane 0,25 111-18-1 Tetrachloroethene 0,15 I 141-18-9 1,3-Dichloropropane 0, 25 114-48-1 Dibronochloronethane 0.75 106-93-1 1,2-Dibroaoethane 1 I 108-90-7 Chlorobenzene 0.15 630-20-6 1,1,1,1·Tetrachloroethane 0.15 75-25-1 Bronoforn 0,5 79-31-5 1,1,1,2·Tetrachloroethane 0.75 I TQL· Target Quantitation Linit· subject to I change due to instrunent sensitivity T· Tentatively Identified, not confirned B· Estinated value O· Samples analyzed for this conpound but I not detected N· Sanple not analyzed for this co1pound O· Detected below quantitation linit I K· GC/KS Analysis perforGed I COHHEHTS • I BHNR/DEH LABORATORY VOLATILE ANALYTICAL REPORT ANALYSIS RESULTS SUPERVISOR~ DATE ';is '1.3 ENTERED BY , . CHECKED BY DETECTED CASI VOA TARGET COMPOUND DETECTED u 1 u 1 u 96-18·4 1,2,l·Trichloropropane 0,25 u u 108-86·1 Broaobenzene 1 u u 95-19-8 2-Chl orotol uene 0. 2 5 u 0, 41 T 106-13·\ 4 ·Chlorotol uene 0.25 0 u 541-73·1 1,J·Dichlorobenzene 0,25 u 0, 51 T 106-46·7 1,4-Dichlorobenzene 1.25 6, 1 u 95-50-1 1,2-Dichlorobenzene 0,25 0. 28 T u 96-12·8 1,2-Dibrono·l-Chloropropane 1 u u 120-82-1 1,2,l·Trichlorobenzene 0, 2 5 u 0 81-68-3 Hexachlorobutadiene 0.25 u u 81-61·6 1,2,3-Trichlorobenzene 0, 75 u u 1634-0\·\ Methyl-tert·butyl ether 5 0 u 71-13-2 Benzene u u 108-88-3 Toluene u u 100-11-1 Ethyl benzene D T u 108-38·3 G,p-Xylenes D u 95-17·6 a-Xylene u u 100-\2-5 Styrene u u 98-82·8 Isopropylbenzene u u 103-65-1 n-P ropy lbenz en, u u 108-67-8 1,3,5-Trinethylbenzene u u 98-06-6 tert·Butylbenzene u u 95-63-6 1,2,l·Trinethylbenzene D T 0. 81 T 135-98-8 sec-Butylbenzene u u 99-81·6 p·isopropyltoluene u u 101-51-8 n·Butylbenzene 1. 6 T u 91-20·3 Naphthalene 3, l other purgeables detected Detected (up to 10 highest peaks! ug/1 --------V d I 111 d -------;( ; ·,, ,--. I )' ~ uAo ,io 2 G 7& I\ T. 3501{:\1Q ·:z ·K8s EA I AL LONG. NO. /~Yk Department of Environment, Healllt, and Natural Rasourcos zo "s.•-.,; 0,) /I Division of Environmental Mana-;iement Groundwater Field/Lab Form LAB NUMUEA 8 L ~ ~ ( J -=) DAT~ REcl£'S/ lo jtz3rimo '.zS llG noc d by: :':) rrom: UL~ to: ArlO, mo, ,:;;;I nno e;, . Jpor I GHAlti]fE:~M§~RDY wano, w;no, Other -------cc;,:c----~-=-- SflO, Kinslon FO O!hor ippod by: Gus, Qr., Olher ______ _ ~ ROUTINE O EMEllGENCY 0 DAT A ENTRY BY: ~ CK Rf; G 3, (•J : I DATE REPORT E O: __ ..:..e::..:":.._L'-1 '------ LLE c TOA( s J: 01¼ /1,,, (r1,b {/le, DATE :LO ANALYSES 400 Spee. Cond. g,1 __ a12s0 c ilp. 10 oc Odor ,oarance Tasia Id Analysis By: IJOIIA/011Y ANALYSES 8001,JIO mg/I X COO Hlori '" mo /I COD Lo.-JJ5 m g/1 Coll/01m:1,H f •c ,1 l 16 115 / I UOml Colllo1m:Uf Toh I l 150 4 / 100ml f oc 6 a o moll T ufbl d I I 1 16 HTU pH '°' unl 11 ,',, lk • I lnl I 1 to pH ~.5 <10 moll ,',,lk1lfnlly '" p/1 l.l "' mo// C11bor11 I• .. ' mo/I Blcarbon11e HO moll 7 Aiunlc;To1,I 1002 """ Cubon dlo,lrh '°' mg/I ,( Chlorld• >l◄O mo/I Chromh,m:tt,, 10J1 uo /I Colo,:111.,. •o P1·Co CJ• otd, "" n,g/1 Comrnenl1; l,JoO PURPOSE: BASELINE, COMPLAINT, COMPLIANCE, LUST, OTHER (cl1cla on.) Ownor C /. n r .k) f'-L v//,Jc s ±,JC ·s'f,7] I Locarion or sllo Oescrlpllon al sarnplino polnl s amp/ i ng Me th od --,.;-::B=-01:'-'1·r..,"2,.:::~,;-::-,:--:-,.._---------( p urn p, bollor, ok.l Remarks Dr·; buecl' ( L.-!-:l i<-' )OOt-<(<C.,( :Ja. r>,,a 1,-.,.I {'-~ r',1 fc c in I ·' Olu. Solid, 70]00 '5 mg/I "'o · Sllwer IOT 1 fluotl<U "' mo/I Al Al!xnloum I I 06 H ■rdn,..a;To1,r 000 moll ,'<' •• B11Lum ·1001 fS ~ Hudn1u (non-cub) "' m·o/1 C• CI I c I um . " Pht nol 1 l 21]0 """ Cd C1dmlum 1027 Sp.clllc Cond. " ul-lho1/cm7 Ch1omlum:Tol1I I OJ ◄ Sull ■ I • '., molt Cu -Copp,, 1 0 4 2 SullJch ,., mo/I ,. · 1,on 10◄5 --Sample 0c., fer ±t..cH (pumping lime. air (;, r;;,.? c·1 1-r 'r C.,/ lemp,7etc.) uo/1 uo/1 0fQlf\Ol)hOll)l':OIUI f'lt!loldll """ mo// Acld HudlCld•• UOII ug/1 u11/I uo II ·y· ' H11 · L{ercury 11~00 L 0--' u11 /I K · Po1111lum 11]1 mg/I Mo -IJ1on11lum snr m.,, 1,2 • Olb1omo~lh1n■ (EO!I} ""' '-l•n~•"••• IO 5 6 UQ/1 , .. Sodium "' mg/I -""' .. " 6" /). a J moll "' HI c ~ • 1 1 0 fi 7 UQ/1 IKH .. " '" moll V '" L • • d IO 5 1 --<'.. 10 UQ/ J H01 ._ HO] 11 H 630 /), OI ' moll s. S1l1nlum 11 ◄ 1 ug /I I P:loltl •• p 6115 mall '" Zinc 1097 u11 /I V - for Dlssotvod Analysl& -submit !Utorod G<Hnp!A nnrl wriln -rn..----·1 b/rv.k ,_ I EHNR/DBK LABORATORY I VOLATILE ANALYTICAL Rl!PORT LAB KO. JG 703 I REPORTED BY •mmo,fl/;_ CH!CI!D BY ~ DATE S, :UJ · R!VIEl'!D BY 1 !RTERJD BY r'/7 CH!CUD BY I SAMPLE TTPI: VATIIR ANALYSIS RESULTS C.1.SI VOA TARGET COMPOURD TQL DETXCTED C.I.S# VOA TARGET COMPOUND DET!C!!D I uo l u l u l 75-JH 1,1-Dichloroethene 0.75 u 96-18-! 1,2,3-Trichloropropane 0.25 u I 75-09-2 Methylene Chloride 0.25 u 108-86-1 Broaobenzene 1 u 156-60-S trans-1,2-Dichloroethene 0.75 u 95-49-8 2-Chl orotol uene 0.25 u 75-31-3 1,1-Dichloroethane 0.25 u 106·!3·4 4-Chlorotoluene 0.25 u 590-20-7 2,2-Dichloropropane 0.25 u 511-73-1 1,3-Dichlorohenzene 0.25 u I 156-59-l cis-1,2-Dichloroetbene 0.25 u 106-46-7 1,4-Dichlorobenzene 0.25 u 67-66-3 Chlorofon 0.25 u 95-50-1 1,2-Dichlorohenzene 0.25 u 74-97-5 Bro1ochloro1ethane 0.75 u 96-12-8 1,2-Dibroao-3-Chloropropane 1 u I 71-5H 1,1,1-Trichloroethane 0.25 u 120-82-1 1,2,!-Trichlorobenzene 0.25 u 563-58-6 1,1-Dichloropropene 0.25 u 87-68-3 Rexachlorohutadiene 0. 2 5 u 56-23-5 Carbon Tetrachloride 0. 75 u 87-61-6 1,2,3-Trichlorobenzene 0.75 u I 107-06-1 1,1-Dichloroetbane 0.25 u 1634-0!-4 Methyl-tert-butyl ether 5 u 79-01-6 Trichloroethene 0.25 u 71-!3·2 Benzene 1 u 78-87-5 1,1-Dichloropropane 0.25 0.31 T 108-88-l Toluene 1 u I 75-27-! Bro1odichloro1ethane 0.25 u 100-41·! Ethyl benzene 1 u 74-95-l Dihro101ethane 1 u 108-38-l 1,p-Xylenes 2 u .10061-01-5 cis-1,3-Dichloropropene 0.25 u 95-47-6 a-Xylene 1 u 10061-02-6 trans-1,3-Dichloropropene 0.25 u 100-42-5 Styrene u I 79-00-5 1,1,2-Trichloroethane 0. 25 u 98-82-8 Isopropylbenzene u 117-18-4 Tetrachloroethene 0.25 u 103-65-1 n-Propylbenzene u 142-18-9 l,l-Dichloropropane 0.25 u 108-67-8 1,3,5-Triaethylbenzene u I 124-48-1 Dibro1ochloro1ethane 0.75 u 98-06-6 tert-Butylbenzene u 106-93-! 1,2-Dihroaoethane 1 u 95-63-6 1,2,4-Triaetbylbenzene u 108-90-i Chlorobenzene 0.25 u 135-98-8 sec-Butylbenzene u I 630-20-6 1,1,1,1-Tetrachloroethane 0. 25 u 99-87-6 p-isopropyltoluene u 75-15-2 Broaofon 0. 5 u 104-51-8 n-Butylhenzene u 79-31-5 1,1,2,2-Tetrachloroethane 0.75 u 91-20-3 Naphthalene u I ' TQL· Target Quantitation Liait-Subject to other purgeables detected Detected change due to instruaent sensitivity (up to 10 highest peaks) ug/1 I T-Tentatively Identified, not confiraed !-Bstiaated Value ORB URID!RTIFIBD PBAl DETECTED BY u-saaples analyzed for this coapound but GC/P!D. I not detected R-saaple not analyzed for this coapound D· Detected below (!Uantitation li1it K-GC/KS Analysis perfoned · I COIOOHTS: 11 I I I I I I I I I I I REFERENCE 24 I I I I I I I I I I .. I I I I I I I I I I I I I I I I I State of North Carolina Department o' ...,nvironment, Health and No .... Jral Resources Mooresville Regional Office Jomes B. Hunt, Jr .. Governor Jonathon B. Howes, Secretary Vivian Burke, Regional Manager DIVISION OF ENVIRONMENTAL MANAGEMENT July 13, 1993 CERTIFIED MAIL RETURN RECEIPT REQUESTED Mr. Barry Sigmon A.A.A. Enterprises, Incorporated Route 14, Box 350 Statesville, North Carolina 28677 RE: Notice of Violation Dear Mr. Sigmon: 15A NCAC 2L Classifications and Water Quality Standards Applicable to the Groundwaters Sigmon Septic T1;ink Service ('°~[i.&r'.{~~jif Groundwater Incident N' 3422 · "" Iredell County, N.C. On August 9, 1990 you were issued a Notice of Violation (NOV) from the Division of Environmental Management (DEM) for violation of the North Carolina Groundwater Standards (15A NCAC 2L .0202). In the NOV you were required to determine the vertical and horizontal extent of soil and groundwater contamination and to submit a site assessment report within 60 days of receipt of the NOV. The NOV was held in abeyance pending a review by the Hazardous Waste Section of the Division of Environmental Management. In April of 1993, the Hazardous Waste Section concluded that the site did not fall under its jurisdiction. On May 5, 1993 staff from the Mooresville Regional Office Groundwater Section resampled two of the monitor wells at the subject site and found that groundwater standards violations still exist at the site. Specific violations are as follows: 919 Nortti Main Street, Mooresville. Nortti Coolina 28115 Telephone 704-663-1699 FAX 704-663-6040 An Equal Opportunity Affirmative Action Employer 50't recycled/ 1 O't post-consumer paper I I I I I I I I I I I I I I I I I I AAA Enterprises, Inc. July 13, 1993 Page Two Constituent dissolved solids nitrate mercury lead 2-chlorotoluene 1,4-dichlorobenzene benzene 1,3,5-trimethylbenzene n-butylbenzene naphthalene Concentration* 650,000 54,000 29 75 2 6. 1 2.3 1 1 . 6 1 . 3 * 2L Standard 500,000 10,000 1 . 1 50 ND 1 . 8 1 • 0 ND ND ND * Concentration in micrograms per liter (parts per billion). ND Not permitted in detectable concentrations. The Groundwater Section staff also sampled two downgradient water supply wells in February of 1993 and found that both wells contained nitrate levels above the groundwater standards. You are responsible for causing the continuing violation of the underground water quality standards because you have stored and/or disposed of septage waste in unlined lagoons. According to 15A NCAC 2L .0106 (c)(1), you are required to assess the cause, significance and extent of the violation, submit a plan and schedule for eliminating the source and for restoration of the groundwater; and implement an approved plan in accordance with a schedule established by the Director. In establishing a schedule, the Director shall consider any reasonable schedule proposed by the person submitting the plan .. To achieve compliance with the above-cited laws or rules, you are required to submit within sixty (60) days from receipt of this letter a site assessment report in accordance with the enclosed guidelines. This data will then be used to submit a corrective action plan which will be due within sixty (60) days after the site assessment report is submitted and approved by this Office. In addition, 15A NCAC 2L .0106(b) states that any person conducting or controlling an activity which results in the discharge of a waste, hazardous substance or oil to the groundwater, or in proximity thereto, shall take immediate action to terminate and control the discharge, mitigate any hazards resulting from exposure to the pollutants and notify the Department of the discharge. To comply with this section of the rules, you must provide an alternate drinking water supply for the residents who use the wells at Route 14, Box 356 and Box 357 (the last two wells on the dirt road behind your facility) within seven days of receipt of this letter. I I I I I I I I I I I I •• I I I I I .,., .. , :fu?EnEerp;},.~_lI!;~.;-;:_fnc. July·13;-·1993_ Page Three You should be aware, however, that the above violation of 15A NCAC 2L may subject you to a civil penalty assessment under the authority of G.S. 143-215.6a of up to $10,000 per rule violation. each day that the violation continues may be considered a separate violation. Failure to respond within the time specified and to voluntarily achieve compliance may result in a recommendation for enforcement, the issuance of a Special Order against you under the authority of G.S. 143-215.2, or a request to the Attorney General to institute an action for injunctive relief. Your response and/or questions should be directed to Chris DeRoller of the Mooresville Regional Office at (704) 663-1699, ext. 235. Sincerely, Mf~ih Brenda J. Smith, P.G. Regional Supervisor cc: Groundwater Section, Raleigh Laurie Martin, Hazardous Waste Section Julian Foscue, Solid Waste Section Rhonda Morgan, Well user Bill Munford, Well user Enclosures: Site Assessment Guidelines Sample Results I I I I I I I '] u I I I I I I I I VOLUME,III REFERENCES