NCD062555792_19980930_Sigmons Septic Tank Service_FRBCERCLA PA SI_Combined Preliminary Assessmen Site Inspection - Volume IV Appendix A-OCR

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STATE OF
NORTH CAROLINA
Department of Environment
and Naturol Resources
Division of Waste Management
Supe,fund Section
COMBINED PRELIMINARY ASSESSMENT/SITE INSPECTION
VOLUME IV
Sigmon 's Septic Tank Sen,ice
NCD 062 555 792
Statesville, Iredell County, Norlh Carolina
Reference No. 06611
September 1998
Donna J. Wilson
Environmental Chemist
Division of Waste Management
Supe,fund Section
~CDEHNR ·(: JI ·Di.visic~a --,f Waste 1Vlanagcmcnt
Organics Lab: V
!norganics L:-1b: __ \I ll'iz Superfund Section
D Hazardous Waste Section
,. D Solid Waste Section ., CHAIN OF CUSTODY RECORD
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Project Name: S~/YluflS '5::efQ'L ;?,1.,l/c.... Sampled By: t~,11¥\.... ltlr' ls.ov. Site ID # (NCD#) N e.-1) cf, Z-5~ 7q -Z... Sampler ID
Location: S-faf-e;,,, i I ( <'.. /\JC Telephone:(ffij 7 33-7-R;o/ -qd-3(7 Address: rz.1.o '3 CV-hi I;.___ /2.d. Date Sampled: 'f3 /zs/ '!1 , '"o[_u(q7
' Time Sampled:
Sample Types: Soil \Vater V Waste Other
Remarks: /5 'YlQ of' 4..5.f c'[ / fc. Sit &f-f es fv be--/yz-,/_ /1 .s +. r, -e j_ -to I nor v,t'I. I\IC.f )A0 -h,r DH -tcs.+ u
Field Sample ¥-01-o ?DJ "'0'2.D 3C4-'t '2,c, ?D.S. 'tw ~ 1>·2.o ·2:,..:i7 lj(
o'UD~~ o'l-O??'f Numbers O"Z-<D::). O 0'20 :>( ( D?o::, ~(c.-020::;i?, D7-0."'o./4 o--i.o::>,( S ~ C52c --:e,f b
0<..() -YJ >i'-o?..o ~1"3 * 020·-,,,11_ -¥-D '2.-o'.:s '2(:)
Relinquished Byl VAA/7}} f) t ~✓.a .A ll . 'iJl ,~7 Date: .,'-Cv 7 Time: LS70
rsl.laturc) -~ ,...--'\ . I
Received By: ~ w/. OfJ r ~(L (l Date: k'-28' -f?Time: /$0 . , (Signature)
Relinquished By: Date: Time: /SiPnaturc)
Received By: Date: Time:
(Signature)
Relinquished By: Date: Time: (SiPnaturc)
R.eceived By: Date: Time:
~Signature)
I
Results Re~ ortecl: ~~-\0. po r1)( Date o//23/fJ Time: '-((, ign'aturc) • I I --1.:1 ·· I
r..')N.c'. 'c'ian,·,.:.,.,: o: E ... ;,os,oo,.,,
' l!c.il1:., & i·hilura\ H.csou~cc~
So!id \Vaslc r..,anagcmcn· Oivi~ion
SAMPLE ANALYSIS REQUEST State Laboratory or Public Health
P.O. Box 28047, 306 N. Wi:mir.gton Street
Raleigh, North Carolina 27611
.. c Number /VC.,G ~ 2--sS5 712-
Name of Site 51:Jmo/lS sqn'c..-7??./1./C...
Field Sample Number ___ _;,O::....::Z0:....::.,,,3o_3=· ""'--------
Site Location_...,S,-,:.f qfey::..:e-'=>'-'//C.!/-''('-'hc:ce_=----------
I Collectc<.! By J S ID# Date Collected e{'z.Jo { q1 Time /4-30
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds . Results(mg/1)
I Environmental Concentrate Comments Arsenic --JYPi I cb&, (.)J-e/, ( Barium
JL: Ground water (1)
--
Solid (5) Cadmium --
I Chromium
S::>--o l -Pu.i --
__ Surface water (2) _ Liquid (6) Lead --
-it-Dtii~~iUt wttttK--
__ Mercury
I _ Soil (3) _ Sludge (7) Selenium --
Wtu..,~
Silver --
_ Other (4) _ Other (8) ·--
I
, __
--
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
~P&T:GC/MS Arsenic benzene ----
V Acid:B/N Ext. Barium carbon tetrachloride ----
MTBE Cadmium chlordane ----PcB --(,,,.-~0,11()(7/ --Chloride chlorobcnzene --Chromiwi! . chloroform ------
I --__ Copper o-cresol --
----Fluoride m-crc~ol --
Iron __ p-cresol ----Lead cresol
I ------
--__ Manganese 1,4-dichlorobenzene --
--__ Mercury --1,2-dichloroethane
Nitrate __ 1,1-dichloroethylene ----I Selenium 2,4-dinitrotoluene ----
Silver __ heptachlor --
Radiochemistry --Sulfates hexachlorobenzene --
I ..... ,_, _____ Zinc hexachlorobutadicne
Par:!meter ----Results (PCi/1) pH hexachloroethane ----
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I Gross Beta. TDS r..itrobcnzcnc ------TOC __ pentachlorophenol --__ pyridine --
I Microbiology --__ tetrachloroethylene
--__ trich!oroethylene
Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol --
--__ 2,4,6-tr:chlorophenol --__ vinyl chloride ----endrir., --
f-2 f'f?//k Rep~L -,,} ~, Z:::/ll~ lindane
I Date Received
--
:nethoxychlor
f?l!J3; l,-~'1-17VA Bl)
Date R{Jirted
,·--toxarhcnc
9~~.3-tf] --
D.,te Extracted jJ-4 B t; ,11£tr;,../4 --2,4-D
I /Jt!/Jftj-;J..-9:?YP ·373409 J:Fif]$ 0silvex)
Date Analyzed8,IJA 9-,J,·97A,,Q Lab Number -· -(j 9-c/ 7 '5[2.~
!)J JS JI 1) I (!t,~viscd 2/91) .. '"
I N.C. r)cr,artr.:c11t of Environl\:.::n1,
' I lca'11;1: & N~tura\ Rcsourca
Solid Waste Management Divis;on
SAMPLE ANALYSIS REQUEST State Laborulory of Public Health
P.O. Box 28047, 306 N. Wilmiiigton Street
RB!cigh, North Carolina 27611
-pte Number Alco Dr;; z.._ sS5 71 z... Field Sample Number ___ _:0=---="Z-6~3£_J_f,_-_____ _
-

-
Name of Site,_St.,_ij-"l'. Lrn-"o"-'//'-'--=S'--~>17qccf,_:,_•--=c.,=---_,72c_:a::,,,_/1-'-'fo'---c__--Site Loeation, _ _;SS,.Li:C¼='-'""-'v:'-'1'---',__//_0/ e_=-----------
1 Colleete_d By_~-~h~7,,--~---ID# ___ Date Collected_0__,_/;_z~s/L_q_7 ____ Tinie _ __,_/__,7'-'S"'--=3:___
I Agency: Hazardous Waste Solid Waste Vs uperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
JlMeS L,u(:{/
Barium --
-V Ground water (1) Solid (5) Cadmium --
I
Chromium
~--0 7--PL-u --
__ Surface water (2) _ Liquid (6) Lead --
_ Sludge (7) ~&--//Jf-.i~§-: WAV::1--,
Mercury
I _ Soil (3) --Selenium --
Uv8if ~ Silver --
_ Other (4) _ Other (8) 6 11°.m., · 1 "<!:l>: e. • 1"(1'1 • \ --
I
--
--
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/I)(mg/kg) Organic Compounds Results(mg/1)
_P&T:GC/MS Arsenic benzene ----
v Acid:B/N Ext. Barium carbon tetrachloride ----
MTBE Cadmium chlordane --fC13 ----
___i.L ,..o,oopJ Chloride ehlorobenzene ----
Chromium chloroform
------
I --Copper o-cresol ----
--Fluoride m-cresol ----, Iron __ p-cresol ----__ , Lead cresol
I ----
--__ Manganese --1,4-dichlorobcnzene
__ Mercury __ 1,2-dichlorocthane --
--Nitrate __ 1,1-dichlorocthylene --I Selenium 2,4-dinitrotoluene ----
Silver __ hcptachlor --
Radiochemistry Sulfates hcxaehlorobenzene ----
I ...... _. Zinc hexaehlorobutadiene ----
Parameter Results (PCl/1) pH hexachloroe:hane ----
__ Gross Alpha --Conductivity __ methyl ethyl ketone
I Gross Beta TDS nitrober.zene ----TOC __ pcntaehlorophenol --__ pyridine --
I Microbiology --__ tetrachioroethyiene
----!richloroethylene
Paramclt:r R,·sults (Col/lOOml) __ 2,4,5-triehlororhcnol --
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --
Dille Received f/'r 2f;.-q7ttlh Reported by
lindanc
I
--
--mcti,oxychlor
~ 8-.,2-9-'977//;6]) --loxaphene
Date Extracted ~ ,g_,_, q1Kt.,<10 Date Reported 2,4-D
P!B~-9~-97-VP 973410
__ 2,4,5-TP (Silvex)
Dale Analyrcd~ Lah Number
I)! IS JJIJI (Revised 2/91)
--I
I N.C.-_Dcpart·:iicnt of Environment,
I lcalth, & Natural Resources
Solid. Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
l9tc Number...:./vi-=-[,=l)'-=-a?;-=-=2..-=---=S=-S--=5_7;__,,.C/_Z..._. ___ Field Sample Number (:) Zo3D5
I
Name of Sitc_';l....z.,~q:.1'11.=0:c..t1,..,S::.
1 --=Y'fq::..:n.:...'--=e.-=--]4.cl· ~11'-'-'-/c..-'-_ Site Location S1q./-esV! //e_
Collected By ~ ID# ___ Date Collected CfJ/zS/'11 Time __ f~7_(_2-__
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds
----
Sample Type Inorganic Compounds Results (mg/I)
I Environmental Concentrate Comments Arsenic --
~ffe re/ W ( (
Barium
VG round water (1)
--
Solid (5) Cadmium --
I ~~{AiK1N<r l!A7cf-
Chromium
__ Surface water (2) _Liquid (6)
--Lead
fJ.-.;B-,ljJ-
__ Mercury
I _Soil (3) _ Sludge (7) Selenium --
ayt f-/1.;rt IM. f>lft"--
Silver
_ Other (4) _ Other (8) f:rL tw/l ----
I ss-o?,-f:w --
--
Organic Chemistry Inorganic Chemistry --
I Jlarumeter Results(mg/1) Parameter Results (mg/1) (mg/kg) Organic Compounds Results(mg/1)
_ P&T:GC/MS Arsenic !,cnzene ----1L Acid:B/N Ext. Barium carbon tetrachloride ----
MTB~ Cadmium chlordane
LL' fCI ----
<O.O«J/ Chloride chlorobenzene ----Chromium chloroform ------
I --__ Copper o-cresol --
--Fluoride m•crcsol ----Iron p-cresol ------Lead cresol --I ----
--' __ Manganese 1,4-dichlorobcnzcne --Mercury 1,2-dichlorocthane ----Nitrate __ 1, 1-dichloroethylcne --I --Selenium 2,4-dinitrotoluenc ----
Silver heptachlor ----
Radiochemistry Sulfates hexachlorobenzene
I
----
······--· Zinc hexachlorobutadicnc
Parameter Results (PCl/1) ----_pH hexachioroethane
__ Gross Alpha __ Conductivity methyl ethyl ketone
I --Gross Beta TDS --nitroben1..ene ----
--TOC __ pentachlorophenol
--pyridine --
I Microbiology __ tetrachloroethylene
--__ trichloroc:hylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenoi --__ 2,4,6-trichlorophenol
at= --
----vinyl chlo,ide
endrin --lindanc
Dale Received '{2f/-C/ 7'14: Reported by I --__ methoxychlor
./Jr.BJ "?-.,;:J.'l-97-v'/3.lJJJ __ toxaphcne
Dale ExtractcJ ~-J.-1,'/114<, •& Da:c Reported 2,4-D --
I ft!sr 9-:2.-'97-VP --2,4,5-TP (Silvcx)
Date Analy,cd ~~1'1. 'l_-~.;:;-7.(!JIJ La!, Numbcr_9_7:ltij 1
DJ IS 3191 (Revised :!/91)
--
I N.C.~)cpart:n~nt of Environment,
1 lcalth, & Natural Resources
Solid -.Vastc Management Division
SAMPLE ANALYSIS REQUEST
sS5 712... Field Sample Number
State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmingtor Street
Raleigh, North Cerolini. 27611
Q?,,o31:¥.:, pte Number Alco Ct;; z_
Sides Vi l /e___ Name of Site <::._; r r S<fti'c__. 74/l/c.. · Site Location grno/lS I Collected _By --JS ID# Date Collected <f(zr,, (17 Time t._o3S
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concen Ira le Comments Arsenic --
Poif.s we(/
Barium
V Ground water (1)
--
_ Solid (5) Cadmium --. --
I + b ~Nt--i!V4-
Chromium
LUI/-TOC --
__ Surface water (2) _ Liquid (6) Lead --
WfLL.
__ Mercury
I _Soil (3) _ Sludge (1) --Selenium
5<;.--c4-Pw Silver --
_ Other-(4) _ Other (8) ----I . --
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Org1•.nlc Compounds Results(mg/1)
P&T:GC/MS Arsenic b1·nzene
' 1./ Acid:B/N Ext. ----
Barium carbon tetrachloride ----
MTBE Cadmium chlordane ----fC/3 --v <C,000/ Chloride chlorobenzene ----
Chromium chloroform ------
I --Copper o-cresol ----
--Fluoride --m•cresol --Iron p-cresol ----Lead cresol ----I --... Manganese 1,4-dichlorobenzene ------• __ Mercury __ 1,2,dichloroethane --Nitrate __ 1,1-dichloroethylene ----I Selenium 2,4-dinitrotoluene ----
Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----
I ······-·· Zinc hexachlorobutadiene
Results (PCi/1) ----
Parameft:r pH hexachloroethane ----
__ Gross Alpha --Conductivity __ methyl ethyl ketone
I --Gross Beta TDS nitrobenzene ----TOC __ pentachlorophenol --__ pyridine --
I Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Para1nctcr Results (Col/lOOml) __ 2,4,5-trichlorophenol --
--__ 2,4,6-trichlorophenol ----__ vinyl chloride ----endrin --
f.-.2f~'f z/,/k) Reported by
lindane
I D2tc Received
--__ methoxychlor
rfr:6} iJ"--..)e,-111/~Bt> toxaphcne --
Date Extractcd[-ylJl-e,-i.] ::J1 rel!',~ Date Reported --2,4-D
I ~.; ?x-97 lf' 973412 _ 2,4,5-TP (Silvex)
Lab Number Dale Analyzc<l&A 9--l-9?6 --
DIIS Jl1J\ (llcviscd 2/91)
I N.C '1;)cpart-.,u;nt of Environment,
I lc:iltt:, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory or Public Health
·P.O. Dox 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
pc Number IV<.)) Or;; Z--sS5 712... Field Sample Number OZ.030]
Name of Sile ~rno/1.S ~kc..-?a./t/C.. Sile Location Sid-es(/( lie..
.I Collected By f,-z_ ID# Dale Collected 9/z(J)(q1 Time /7U3
I Agency: Hazardous Waste --Solid Waste Vsuperfund TCLP Compounds
Sample Type Inorganic Compounds Results (mg/I)
I Environmental Concentrate Comments Arsenic --
VGround water (1) /nD/l/7'Jr we If ()//Sr' /z. Barium --
_ Solid (5) Cadmium --
I Chromium
ss-os-G-w --
__ Surface water (2) Liquid (6) Lead --__ Mercury
I _Soil (3) Sludge (7) --Selenium
Silver
_ Othen(4)
--
Other (8) --
I ----
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
. P&T:GC/MS Arsenic benzene .,------
L/ Acid:B/N Ext. Barium carbon tetrachloride ----
MTBE Cadmium chlordane ·--PU3 ----
V <:.o. "oo t Chloride chlo,obenzene ----
. Chromium chloroform ------
I --Copper o-cresol ----
--Fluoride m-cresol ----
Iron __ p-cresol
----Lead cresol --I ----
----Manganese --1,4-dichlombenzene
., __ Mercury 1,2-dichloroelhane ----
--Nitrate __ 1,1-dichloroethylene --I Selenium 2,4-dinitrotoluene ----
Silver __ heplachlor --Radiochemistry Sulfates hexachlorobenzene ----
I ······--Zinc hexachlorobutadiene
Parameter Results (l'Ci/1) ----
pH hexachloroelhane ----
--Gross Alpha --Conductivity __ methyl ethyl ketone
I Gross Beta TDS nitrobenzene ------TOC __ penlachlorophenol --
--__ pyridine
I Microbiology --__ letrachioroethyiene
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenoi
----__ vinyl chloride
endrin --
Dale Received ?: 2.f,,.-P7~ Reported by
lindane
I
--__ mcl,wxychlor
/;4E11[-,,l. 9 -97¥ 6' 8D __ toxaphene
Date Extracicd/!f\A (J,Lq .C,, fL.tL1 C/4 Date Reported --2,4-D
' 973,ii:J I /Jey;. 9'""< -97-i4> --2,4,5-TP (Silvcx)
Dal c Analy1.cd (3,!,/1'! q_.,2_,£ z Ail Lah Number
DI IS 3JIJ! (Revised 2/91)
--
I . N.C.·I?c~LJrt-:iv;.nt of Environment,
I lcalth, & Natural Resources
Solid Waste Management Division
.. le Number NC,Q Q-;; Z...
SAMPLE ANALYSIS REQUEST
S-55 712.. Field Sample Number
Stale Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh,_ North CaroiiM 17611
0'2..03£.:6
-Name of Site SJ3mo/1S Scfkc... 7a,/l/C.. Site Location S1des Vr '! le.-
I Collected By JS ID# Date Collected '?J{z.& (ci 1 Time /3/0
'
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
//II Cf/ 1'-!ur t,ue((
Barium
V Ground water (1)
--
.. Solid (5) --Cadmium
I off;,;72--ttJ,v i c{ ::$),
Chromium --
Surface water (2) _Liquid (6) Lead --
SS-Ob-CrW
Mercury
I _ Soil (3) · Sludge (7) --Selenium --Silver
_ Other,{4)
--
_ Other (8) --
I ----
Organic Chemistry Inorganic Chemistry --
I Purumeter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organlr: Compounds Results(mg/1)
... _ P&T:GC/MS Arsenic benzene
.• Acid:B/N Ext. ----Barium carbon tetrachloride ----
MTBE Cadmium chlordane ------v ?c-B -<O,ODeJ/ Chloride chlorobenzene ----
Chromium chloroform ------
I --Copper o-cresol ----
--Fluoride m-cresol ----
--,:,1 Iron __ p-cresol --··, Lead cresol
I ------,. __ Manganese 1,4-dichlorobenzene
--... --
--__ Mercury __ 1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylene
I --Selenium 2,4-dinitrotoluenc ----
Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene
I ----
······-·· Zinc hexachlorobutadiene ----
Parumet~r Results (PCl/1) pH hexach!oroethane --__ Gross Alpha --Conductivity __ methyl ethyl ketone
I Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol --
--__ pyridine
I Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --
?,-lf'~C/7 ~ Reported by
lindane
I Date Received
--__ metnoxychlor
~ B-t-1,q-1 lc,/r.,.1l7 toxaphcne --
Date ExtractcJ~'j'-.;l-~ Date Reported . . q --2,4-0
PatJs 9~.;i.-9w 9•;341 __ 2,4,5-TP (Silvcx)
Dale Analyzed t!~tl. 'i,-J.c!J.·z Lab Number
])I IS 311JI (Revised 2/91) • --I
I -il-'..C. Ocp:1,r1~1cnl of Environment,
1 !c'altl:; & Natural Resources
Solid '.-/aslc Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmingte,n Street
Raleigh, North Carolina 27611
· . ..,,le Number...:M..=C::.OL-.c:C,f,.,:..,'.Oe::_::z_:__-=s'---s_s=-._7:_,_'1_:_-2-___ Field Sample Number oL0?:iX/
Name of Sile S,,3rno/l.S $:L'fii'c 7?,/l/c.. Site Location SfdeJVi //e__
_Collected By __ ___,J=<-:S;:__ ____ ID# ___ Date Collected <a(zs(ql Time __ ('--.S_I __:s __
I Agency: Hazardous Waste Solid Waste· Vs u per fund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
73e{oCAJ Barium
p?6 --
___ Groundwater (1) _ Solid (5) Cadmium --I Chromium
V Surface water (2) ss-01 -<;,w --
_ Liquid (6) Lead --
--Mercury
I _Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --
I --
--
Organic Chemistry Inorganic Chemistry --·
I-Parumeier Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mr:/1)
P&T:GC/MS Arsenic benzene ----V Acid:B/N Ext. Barium carbon tetrachloride ----MTl3E Cadmium chlordane I. --fC,,B, --:;;o,"oc7 ----
V Chloride chlorobenzene ----Chromium chloroform ----I --_._ Copper o-cresol --Fluoride m•crcsol ------
--Iron p-cresol ----
I --Lead cresol ----
--1(,1. Manganese I ,4-dichlorobcnzene ----
----Mercury 1,2-dichloroethane
I --Nitrate __ 1,1-diehloroethylene --Selenium 2,4-dinitrotoluene --Silver __ heptachlor --
I
Radiochemistry Sulfates hexachlorobenzene ----...... -,.-Zinc hexach lorobutadiene
Parameter ----Results (PCi/1) _pH hexachloroclhane
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Ileta TDS nitrobenzcne ----
TOC __ pentaehlorophenol --
--__ pyridine
•1 Microbiology ----tetrachloroethylene
--__ trichloroethylene
Parnmctcr Results (Col/lOOml) __ 2,4,5-trich\orophenol
~ --
--__ 2,4,6-trich.Jorophenol
----vinyl chloride
endrin --
I ?-2-f:-'171/,y
\indane
Dale Received --Reported by mcthoxych\or
(!,v, f?·H-'11 fLIC,,.,-C, --
--loxaphene
I Dale ExlraclecifClJf'1-_~-"171//J Dale Reported 2,4-0
1-'es!s 9-~-977/P 973415 __ 2,4,5-TI' (Silvcx)
;),'.'.e. ~,'.';:ly,ed ~f,--2-9? 0, Q Lab Number --
N.C. Dcp:irtment of Environment,
I !Callh, & Na1ural Resources
Solid Waste Management Division .
SAMPLE ANALYSIS REQUEST State Laborator)' of Public Health
P.O. Box 280-47, 306 N. Wilmington Stn:.ct
Raleigh, North Carolina 27611
. . l\l,i1e Number Alco ~ z_ s-S5 712.. Field Sample Number O ·z_o3( 0
Name of Sile 'yJ@)0/1.5 St:t7kc... 7q;t /c. Site Location Sf q.fey VI //e...
I . Collected By _____ -J_' _<; _____ JD# Date Collected ?>/z..s/ ct1 Time /4<!)0
----I -!--'=~--
I Agency:. Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
Sample Type ··Inorganic Compounds Results(mg./1)
I Environmental Concentrate Comments Arsenic --
&ck?j muccR Barium --__ Groundwater (1) _ Solid (5) Cadmium --
I Chromium
Vsurface water (2) Po-'\4 --_ Liquid (6) Lead --I Mercury
~-Clfj-f?t,.,SW --
I __ Soil(3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --.
I --
--Organic Chemistry Inorganic Chemistry --
I Purnmeter Rcsults(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
_ P&T:GC/MS Arsenic benzene -----~ • L,,-Acid:B/N Ext. Barium carbon tetrachloride . II ----I ~ MTBE Cadmium chlordane
L,-pee ----<t>•OOC/ Chloride chlorobenzene ----
Chromium chloroform ------
I --Copper o-cresol ----
--Fluoride· m-crcsol ----
--Iron p-cresol ----
I --.. Lead cresol ----·.,,' Manganese 1,4-dichlorobcnzene ------
--,, __ Mercury 1,2-dichloroethane --
I --Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene
I ----······-··-Zinc hexachlorobutadiene
Parameter Results (PCi/1) ----pH ,;,exachlorocthane ----__ Gross Alpha --Conductivity --methyl ethyl ketone
I Gross Beta TDS nitrobenze:i.e ------TOC __ pentachlorophenol --
----pyridine
I Microbiology ----tetrachloroethylene
----trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 7,4,6-trichlo,ophenol
--1----vinyl chloride
I cndrin --
I t'r 2-?-Vtl/4 Reported by
lindane
Date Received --
--mcthoxychlor
f:r/t-6 ,z_q -<(1 t:tc, wf", toxaphcne
Dale ExtraclcJ PCBf"l_-.:l.-97'1(P bate Reported --
I --2,4-D
A:'.Bs 'l-~-'17-YP 973416 --2,4,5-TP (Silvcx)
Date Analy1.cd6!/,12-c,l-<z:i lfJ£). Lab Number
1\1 I<.'. 71U1 f11~.,;,.,.,1 7 /"1\ • --
.·. ffl. N.C., Department of Environment, llJ I kalth, & Natural Resources
Solid Waste Man3gcmcnt Division
._ ..,ilc Number NC.,/) C0 2--
SAMPLE ANALYSIS REQUEST
s-SS 712... Field Sampic Number
State Laboratory o( Public Health
P.O. Box 28047, J.06 N. Wilmington Stn:Ct
R.alei~~. North Carolina 27611
()'20?>( (
I Name of Sile ~rno//S ~-kc_ 74;1/~-Site Location Sid-es vr '/ le..
... ·•.
I
I
I
I
I
I
~ ,,
I
I
I
I
I
I
I
I
._Collccled By _J<;, ID#. Dale Collected c{;/__7--S['11 Time 0/o
Agency: Hazardotis \Vaste Solid Waste Vs uperfund . TCLP Compounds ----
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --
&>ckJro~
Barium --Cadmium __ Ground water (1) ._ Solid (5) --Chromium
V Surface water (2) p.ere t'c/l)tc/ sf.e&-N\_ --
_Liquid (6) Lead --
SS-05 _c->w --Mercury
_·_Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
_P&T:GC/MS Arsenic benzene ----_:k Acid:B/N Ext. Barium carb1,n tetrachloride ----MTBE Cadmium chlordane
l.----f'C-/J <O,ODO/ --Chloride --chlorobenzenc ------Chromium chloroform ------
--Copper O•cresol ----Fluoride m•cresol ----
--Iron . __ p-cresol --Lead crcsol ------, Manganese 1,4-dichlorobcnzcne ------
--__ Mercury 1,2-dichlorocthane
--Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotolucne --Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzcne ----······-··--· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH hcxachlorocthane
__ Gross Alpha __ Conductivity __ methyl cthyi ketone
Gross Beta TDS ni_trobenzcnc ------TOC pcntachlorophenol ----
----pyridine
Micro!Jiolcgy --__ tetrachloroethyleIJc
--__ trichloroethylenc
Parametff Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
cndrin --
Date Received F~ )t,,--97 1/;;h Reported by
lindanc --
--mcthoxychlor
' &1A €,,1-1-q,,uc, .v<'f 973417 --toxaphcnc
D:ite ExlractedA?e.,-9 ~.:l_-971/P Date Reported 2,4-D --
A;,Bj-9-..z-9?VP. __ 2,4,5-TP (Silvcx) --
Dale /\nal11.ed &A1'4 <;-</. 9J .,g,0 Lab Number --
I 0'.C. Dcp:1rtri1c.nt of Environment,
I lc,.ilth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
l'.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
m.ilc N umber_.:M...:._,cc::;.o'--"'..x=-c2--=--=s=-=S-=5=----=-7__,1c_Z...:c..;_c__c..__ Field Sample Number O (__J?) ?> ( 7...
N.ame of Site S(jrno/1 S 5:t:f-h 'c... M/l /c. Site Location Sf qfey Vi //e_
.~ CollectedBy bt\1 ID# ___ DateCollected <J{2<p{q7 Time D'3'2()
I Agency: Hazardous Waste . Solid Waste Vsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic . --
[){tu i c{SG/\ ?00q Barium --
, . __ Ground water (1) _ Solid (5) Cadmium --
I Chromium
V Surface water (2) ':::, ':::,~ (.O -S1AJ --
_Liquid (6) Lead --__ Mercury
I _Soil{3) _ Sludge (7) Selenium --Silver --
. _ Other (4) _ Other (8) --
I --
--Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
_ P&T:GC/MS Arsenic benzene
~ ----L Acid:B/N Ext. Barium ca,b•Jn tetrachloride ----MTBE Cadmium chlordane --f'U3 ----
L,. <O,ODO/ Chloride chlorobenzene ----Chromium chloroform ------I --Copper o-cresol ----
--Fluoride m-crcsol ----
--Iron p-cresol ----
I --' Lead cresol ----
--l'_:, Manganese 1,4-dichlorobenzene ----
----Mercury --1,2-diehloroethane
I --Nitrate __ 1,1-diehloroethylene --Selenium 2,4-dinilrotoluene --Silver __ heptachlor --
I Radiochemistry Sulfates hexachlorobenzene ----
······-··-Zinc hexachlorobutadiene
Paramldcr ----Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity methyl ethyl ketone
I --Gross Beta TDS nitrobcnzcnc ------TOC pentachlorophenol ----
----pyridine
I Microbiology ----tetrachloroethyleue
__ trichloroethylene --Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
--·-
__ vinyl chloride
cnc!rir. --
I Date Received ~ 2 fr--</7 ~ Reported by
lindanc --methoxychlor --ff\A fr /JI Lf 7 /:t:, "1/ --toxaphcnc
I Dale l:.xlraclcd/Jl!.B59-,2--9Z'///' Dale Reported 2,4-D --Pesi-9-~-97-v,,q 973418 __ 2,4,5-TP (Silvcx)
D,dc_An,:ly,cd l¼:4 9. '1:-978',Q Lah Humber --
I ·".C. Dcp;irt~1cnt of Environment,
I lc'alth, & Natural Resources
· Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmir.gtOn Street
R.Blcigh, North Carolina 27611
111,ite Number...:M...:..=t:..:..O'......:c~-"'-z.._=----....:s=----S-=5_7__:_!C/_2... ___ Field Sample Number ____ oS<C-·--z_--=-o-~-"'-'-13=------
Name of Site Si3rno//S 'Sq-kc ----z??,/l/c.. Site Location __ S,.._i_'qj-ey-'-'""-'~'-1'-',.__/~/e__~---------I Collected By __ --'f'-1)_//;__._/ ____ ID# ___ Date Collected_0 ___ /_Z-_G_(,_"f-'--'7 ____ Time CfCfZ.o
I Agency: Hazardous Waste Solid Waste Vs u perfun d TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --0 tMJ I 'q '.Y5t\ VA~
Barium --
__ Groundwater (1) Solid (5) Cadmium --
I I Chromium
. · V Surface water (2) 'bvpliu---k,, --
_ Liquid (6) Lead --I Mercury --
I Soil (3) _ Sludge (T) S,S-//o -SW Selenium --Silver --Other ( 4) _ Other (8) ----'
I --
--Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
._ P&T:GC/MS Arsenic benzene
I --· --t:iL: Acid:B/N Ext. Barium ' carbo:i tetrachloride --Cadmium --MTBE chlordai.c
V PUJ ----<o,opo/ Chloride chlorobenzene ----Chromium chloroform ------I --Copper o-cresol ----
--Fluoride m-cresol --
--Iron __ p-cresol --
I --.. Lead cresol ----~·-Manganese 1,4-dichlorobcnzene ------
----Mercury --1,2-dichlorocthane
I --Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----
'
Silver heptachlor ----Radiochemistry Sulfates hcxachloroben1.ene I ----""··-··--· Zinc hcxachlorobutadiene
Panunetcr ----Results (PCi/1) _pH hexaehloroethanc
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Beta TDS nitrobenzcne ----
TOC __ pcntachlorophenol --
--__ pyridine
I Microbiology --__ tetrachloroethylene
--__ trichlorocthylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-tric!1loropheno!
------vinyl chloride
endrin --
I (-2-f~ Reported by
lindanc
Date Received --mcthoxychlor
~} ---9-3--l/(P toxaphcnc --
I D:itc Extraeiedl/111 q.~q_1 i:,f;_ .. ,fq. Date Reported --2,4-0
/Jee; 9-s-971f 973419 --2,4,5-TP (Silvcx)
Dale I\ naly1.cd £2A.J./12-~~5' Zd-Lab Number
"I I'-.' 'l1<ll /1>-.. :.-.• ,1 "'l /!It\ --
N.C., Dep;1rtr.,ent of Environment,
I lcalth, & Nat_ural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. l3ox 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
..,ite Number..:M-=C:::.O'-=C(.;'-""--2-==--....:S=-....:S-=5=----....:7_1c...._:_2-___ Field Sample Number Q--z.,f) '3/f
Name of Site <;;3rno,1 S Stp-h 'c.... ]a/I /c. Site Location Sf afey Vi '//e__
I _ C.ollected By /)/4J ID# ___ Date Collected 0( 2.S( ql Time ("o /S
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
I Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium Tm-S, '7reY-'v\ --
__ Ground water (1) Solid (5) Cadmium --I t.,ues.f--cP s.i'-/z. Chromium
V Surface water (2) --_ Liquid (6) Lead --
ss~ !b~s1.AJ --Mercury
I _ Soil (3) _ Sludge (7) Selenium --Silver --. _ Other (4) _ Other (8) --
I --
--
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene
",•'· ----.. L---·Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane
v Pee ----<o,oool Chloride chlorobenzene ------
. Chromium chloroform ·------I --Copper o-cresol ----Fluoride m•cresol ------
--Iron p-cresol ----
I --Lead cresol ----
--' Manganese 1,4-dichlorobenzene ----
----Mercury --1,2-dichloroethane
I --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --
I Radiochemistry Sulfates hexachlorobenzene ----······-··-Zinc hexachlorobutadiene
Pararnett:r ----
Results (PCi/1) pH hexachloroethane --
I
__ Gross Alpha --Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobcn1..c.nc ----TOC __ pentachlorophenol --
----pyridine
I Microbiology --__ tetrachloroethylene
__ trichloroethylene --Parameter Results (Col/lCOml) --__ 2,4,5-trichlorophenol ,. ----__ 2,4,6-trichlorophenol
·----vinyl chloride --
cndrin --
I Dale Received f-2-'c-9~ lindane --Reported by methoxychlor --fJe&'s'f-3-17 7J --toxaphenc
I Date Extracted 9'~1 "f ·3 ·0i7 l?IL,t,<,G]_ Dale Reported 2,4-D
fbsl-'1-5-9?-t/p --
973420 --2,4,5-TP (Silvex)
Date Analy-1.cJ (fil/t-11/ -1-976[) Lab Number --
D .~.C. Department of Environment,
I \Ca Ith,' & Natural Resources
So)id Waslc Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 2761 l
--~ite Number-'M_r,,=..,co_D(;::..=~2.-_s_S_.S_?___,_1_2-__ _ Field Sample Number o·-z,e, ~/ ..S
Site Location Sfq}es Vi / /e_ Name of Site S,31110/1 .5 Stp-fi 'c... 7g ;1 /c..
Collected By JS. ID# Dale Collected <o/zs/ '11 Time (72-S
I Agency: Hazardous Waste Solid Waste VS u perfun d TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
C)J c' l{ itLtV\ s. T-)0'1. cl Barium --
__ Ground water (1) _Solid (5) Cadmium
I --
I Chromium
V Surface water (2) <;,s, -/1~ SW --
_ Liquid (6) Lead --Mercury --
I _ Soil (3) _ Sludge (7) Selenium --Silver --
_ Other (4) _ Other (8) --
I --
--
Organic Chemistry Inorganic Chemistry --
I Parameter Rcsults(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
_ P&T:GC/MS Arsenic benzene ----
,____k--Acid:B/N Ext. Barium carbon tetrachloride ----
MTBE Cadmium chlordane .
---.lL': Pcf3 ----
-<t:l,000/ Chloride chlorobenzene ----
Chromium chloroform ------
I --__ Copper o-cresol --
--Fluoride m-crcsol ----
Iron __ p-cresol ----
I --Lead cresol ----
--__ Manganese 1,4-dichlorobenzene --
--__ Mercury 1,2-dich loroethane
--Nitrate __ 1,1-dichloroethylene
I --Selenium 2,4-dinitrotoluene ----
Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene
I ----
. .,.,._ ···-······--···-Zinc hexachlorobutadiene
Paramt:lt:r ----
Results (PCi/1) _pH hcxachloroethane --__ Cross Alpha __ Conductivity __ methyl ethyl ketone
I Gro.s.s Ucta TDS nitrobenzcne ------
TOC __ pentachlorophenol --
--__ pyridine
I Microbiology ----tetrachloroethylene
·---__ trichloroethylcne --l1araml'lrr Results (Col/!00ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --
lindanc
I Date Received ?-k'6-97a~ Reported by
--mcthoxychlor
_ l'(!.8'T 9-3-977/P --
--toxaphcnc
D:1\c E.xtractcd Gt./\ 'l~-3'-"( 1 t:,1(_ Pt.k--7 Date Rcro.tcd 2,4-D
I /lc?LJS-9-5-9?1/'P
--
973421 __ 2,4,5-TP (Silvcx)
D :it c ;\ 11" lyzcd/1;,J_g..!J..-.'f:::_ 978£> Lah Numh<.:r
Ill 1-.: 1.ltJI (I),.,.;.,,,! ,/()t \ --
11 N~C. qcp.ir;tmt!nl or Environment, II I lcallh, & Nalura\ Resources
Solid Waste ManagemCnt Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Str\:ct
Raleigh, North Carolitla 27611
~le Number Ale/) 00 z_ s-ss 71 z... Field Sample Number O 2-0?:1. b
Name of Site S(gmo/1 S 5q:>-fi 'c_ 72<,/l /c... Site Location Sf qfey 1/i '( /e_
• Collected By A z.... ID#_' ---Date Collected Co( zs( 1, Time ( 0(8
·I Agency: Hazardous Waste Solid Waste Vs uperfund TCLP Compounds ----
Sample Type Inorganic Com pounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
s;g N\ol\ ()/e f I
Barium
. V Ground water (1)
--
Solid (5) Cadmium --Chromium
I __ Surface water (2) Liquid (6) *bf--1 fv/Q N(r --Lead
UJA T E:r'& /J.JcLl-1}-
Mercury
_Soil (3) _Sludge (7) --Selenium
I --Silver
_ Other'(4) _ Other (8) '5):,-?,"'Z--PW ------
I --
Organic Chemistry Inorganic Chemistry --
I Pnrameter Results(mg/1) Parameter· Results(mg/l)(mg/kg) Organic Com1iounds Results(mg/1)
_P&T:GC/MS Arsenic benzene ----
L-,-Acid:B/N Ext. ' Barium carbon tetrachloride ----
MTBE Cadmium chlordane ' ----fC./3 --
[.,, <0,00'7/ Chl_oride chlorobenzene ----Chromium chloroform ----
I --__ Copper ' o-cresol --
--Fluoride m-cresol ----Iron p-cresol ------Lead cresol ----I --
--" ___ Manganese 1,4-dichlorobcnzcne --
--__ Mercury 1,2-dichloroethane
Nitrate __ 1, 1-dichloroethylene ----
I Selenium 2,4-dinitrotoluene ----Silver heptachlor ----
Radiochemistry Sulfates hcxachloroben1,ene ----
I ······-·· Zinc hexachlorobutadiene
Parameter Results (PCi/1) ----_pH hexachloroethane --
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Beta TDS nitrobenzene --TOC __ pentachlorophenol --
--pyridine --
I
Microbiology --__ tetrach!oroethylene
--__ trichloroctbylene
P.iramcter Results (Col/lOOml) __ 2,4,5-triehlorophenol --2,4,6-trichlorophenol ------vinyl chloride ------endrln --lindane --
Date Received 'l~2~1/fa--Reportcd by I __ mcthox-ychlor
fee:r 9-3-7-vP __ toxaphcne
Date Exlraclc<lfi'-:ll C/c3:, •'i7 ldt,tNL7 Date Reported 2,4-D --
I f/Jt!BJ. 9-S-'l'7VP 973422 --2,4,5-TP (Silvcx)
Date Analyzed e&,4 9 .. '[_,')_7. ,gJ) Lab Number
1)1 IS Jl1J\ (llcviscd 2/91) --
I\ r,.·.c. l?epar.ment of Environment, IJ I lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
S"S5 7C/Z.. Field Sample Number
State Laboratory or Pu~lic Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
t>Z.o3r7 ~c Number /vC,Q (X;z_
Name of Site ~rno/1.S ~n'c 74/t/C. Site Location S1qkvr lie...
E Collected By .JS ID# Date Collected <o(z~t11 Time /5(6
I Agency: Hazardous Waste --Solid Waste Vsuperfund TCLP Compounds
Sample Type Inorganic Com pounds Resul\s(mg/1)
I . Environmental Concentrate Comments Arsenic --
U/l']bert!A UJe(/
Barium
V Ground water (1)
--
_ Solid (5) Cadmium --
I f-'t:l--1 /Ut:-t Al &-
Chromium --
__ Surface water (2) Liquid (6) Lead --
WA,c:,e. lU el /., f-
__ Mercury
_Soil (3) _ Sludge (7) Selenium
I --Silver
SS-3s--µ,,u --
_ Other (4) _ Other (8) ----
I --
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Co1•11,ounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------
Acid:B/N Ext. Barium carbon tctrc.chloride ----
MTBE Cadmium chlordane --PW <:O,Ot:JO/ ----v Chloride chlorobcnzene ----
Chromium chloroform ------
I --Copper o-cresol ----
--Fluoride m-cresol --,. Iron __ p-cresol ----Lead cresol
I ------
--\;, __ Manganese --1;4-dichlorobenzene
;., __ Mercury __ 1,2-dichlorocthane --
--Nitrate __ 1,1-dichloroethylene --
I Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----
I '"••·-· Zinc hexachlorobutadiene ----
Parameter Results (PCi/1) pH hexachlorocthane ----
__ Gross Alpha --Conductivity __ methyl ethyl ketone
I Gross Beta TDS nitrobcnzcne
------TOC __ pentachlorophenol --__ pyridine --
I
Microbiology --__ tetrachloroethylen;:---,
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-tricnlorophenol
----__ vinyl ci:loride
e·ndrin --
Date Received ~ 2f"-97% Reported by
lindane --
I --methoxychlor
f<:.B~ 9-3-4?-VP --toxaphene
D:ite Extractet!!)tcil c1,3 "11 &tl,,J/ Dale Repoited 2,4-D
I rt:85-9-5-97J/P 973423 2,4,5-TP (Silvex)
Date An,tly1.c<l BNtJ. 'l-i;--9zA£1 Lab Number
1)1 IS 31'Jl (!\cviscd 2/91)
--
-

-
i',.!.C. l?cp:!rtm,;.nt of Environment,
1 lcalth, & Natural Resources
Solid Waste Managcmcnl Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilr.1ington Street
Ralcit,h, North Carolina 27611
ptc Number-'M-'--'=r:,,:..i)'--"~--""-2,,.=---S'---S_5_7___,_C/_Z.... ___ Field Sample Number __ __:b=---cJb-=--_"3_c....c.[-=<z)'--------
, Name of Site_S,_,_g~m"'o"'//-'-"'.5'---=Yf=:....fi_•c...=--_]a..J..:.=-;1'-'-/<_c.. __ · Site Location _ __,S'""'-f qd-ey::...::c:~~~ec/_/c..tcoe__=----------1 Collected. By JS ID# ___ Date Collected __ 't:J__,__7/4__,~~q:....7..:__ ___ Time_(_S4-o_·~'----
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds
----
Sample Type Inorganic Com pounds . Results(mg/1)
I Er.vironmentnl Concentrate Comments Arsenic --Barium
t---Ground water (1) 7e111Je«f w<-t I --
_ Solid (5) Cadmium --Chromium
I * b/2.J N{<::_tfK:r --
__ Surface water (2) _ Liquid (6) Lead --
w eu-* __ Mercury
Soil (3) Sludge (7) IJJATefl-Selenium
I --Silver
s<;.-34---Pw --
_ Other (4) _ Other (8) --
I Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
_ P&T:GC/MS Arsenic benzene ----
v Acid:B/N Ext. Barium carbon tetrachloride ----
MTBE Cadmium chlordane --v fJcJ3 --~-pap/ Chloride chloroben.zene ----
Chromium chloroform ------
--Copper o-cresol
I ----
--Fluoride m-cresol ----Iron p-cresol ----Lead cresol ------I .,, Manganese 1,4-dichlorobcnzene --~:. ----,,. __ Mercury __ 1,2-dichlorocthane --Nitrate __ 1,1-dichloroethylene ----
I Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----
I ··---·~--Zinc hexachlorobutadiene --
Pam meter Results (PCi/1) _pH hexachloroethane --
__ Gross Alpha --Conductivity __ methyl ethyl ketone
I --Gross Beta TDS nitrobenzcne --TOC __ pentachlorophenol --__ pyridine --Microbiology ----tetrachloroethylene
I --__ trichlorocthy!ene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --__ 2,4,6-trichlorophenol ----__ vinyl chloride ----endrin --
Date Received f;. ff-~77 Wleportcd by
lindane --
I __ methoxyehlor
RBS-q-7/-9-n,',o __ toxaphene
Dale Exlraclc<l [JJIA '/·fl._-1'1 UL-· Dale Reported --2,4-D
PeB.5-')~97V.P 973424 __ 2,4,5-TP (Silvex)
Dale Analy,e<l &/19.-l"'-'l.Z ,8..0 Lab Number
l)IIS J\IJl (llcvisccJ 2./91)
--I
I ,'.:.C. Dcp:.irtn_1cn1 of Environment,
1 lc~llh,""& Nalural Resources
Sulid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolin.a 27611
P,itc Number_;_/vi-'t:,=Q"'-'-{)?;-=--'-2--_S_S_5_7_'1,.._Z... __ _ Field Sample Number (') ?_<b~(Cj
· C .' ' .J. I . N" me or Site __ '--/.,_13,q;_m.,_,oe.:;/l..:..;::S:__=Y'f=:../l_'-=c....=-_.Mc='-'-/l-'Cl'-'c. __
I Collected By S, ID#·
Site Location Sfq./e.svr //e_
Date Collected ~1-':,( 11 Time [~7.o
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1) • Environmental Concentrate Comments Arsenic --
&mbc,M Barium &/ow --
__ Ground water (1) _Solid (5) Cadmium --
I p(JY\J Chromium
V Surface water (2)
--
_ Liquid (6) Lead --
Ss.-1/ro---Mercury
__ Soil (3) _ Sludge (7) SVJ Selenium
m
--Silver --
Other (4) --Other (8) --
--
I --
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
--P&T:GC/MS Arsenic benzene ----
v Acid:B/N Ext. Barium carbon tetrachloride ----
MTl3E Cadmium chlordane ----fc.B, --V <O,POO/ Chloride chlorobenzene ------
Chromium chloroform ------
I --__ Copper o-crcsol · --
--Fluoride m-crcsol ----Iron __ p-cresol ----Lead cresol ----E --
----Manganese --1,4-dichlorobenzeoe
Mercury 1,2-dichloroethane ------Nitrate __ 1,1-dichloroethylene ----I Selenium 2,4-dinit rotolucne ----Silver __ heptachlor --
Radiochemistry Sulfates hexachlorobenzene ----
I ···············------·--·----· Zinc hexachlorobut ad iene
Paraml·lcr ----
Results (PCi/1) ;,l-l hexachlorocthanc ----__ (Jross Alpha __ Conductivity __ methyl ethyl ketone
m
Gross Beta TDS nitrobenzcnc ------TOC __ pcntachlorophenol --pyridine --
m
Microbiology ----tetrachloroethylene
--__ trichloroethylene
l'araml'll'r Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
--_·_ vinyl chloride --endrin I --?¥-, f--9?Jte,Reportcd by
lindaoc
E, Date Received --
/'t?l3.f-?-V:-7YP --methoxychlor
toxaphene --
t)atc Extracted biL/1 q,4 -<h,t::--IL. Dstc Reported 2,4-D --
I ,Q:ffe 9·S--P7VP 973425 --2,4,5-TP (Silvcx)
Date 1\n:ily1.cJ _d,UJ q_-~--22 A,[) Lah Nu111bcr -I 'o, ,. --, "" i \J ,.. ,., "' "! foll •
I
I i-J.C. J?cp_:1rtm1~nt of Environment,
I lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N.-Wilmington S:rect
Raleigh, North Carolina 27611
.... le Number--'/vi-"'[."'/)<-.:D(;'-""-..:.z__..:.s;_S_5_;___7::_,_C,_Z.. ___ Field Sample Number b -z_c, ::;Lv
-. NameofSite 5J3rno//S St:(fi's:..-7?J,/l/c._ Site Location S1d-e,svi//e.. I Collected By -!J; ID# ___ Date Collected t:J("2-t>{ '17 Time J?f{b
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
Sample Type Inorganic Compounds Results (mg/I)
I Environmental Concentrate Comments Arsenic --
EqurJ?me~ 11~~4_:l:e.-
Barium --
__ Ground water (1) _Solid (5) Cadmium --I , Chromium
I 12/a"'l --
__ Surface water (2) Liquid (6) Lead --
<;,s---zco -l<.../3 --Mercury
_Soil (3) Sludge (7) Selenium
E --
V Othe,' (4)
Silver
_ Other (8) ----
--
I --
Organic Chemistry Inorganic Chemistry --
•• Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
_P&T:GC/MS Arsenic benzene ----
Acid:B/N Ext. Barium carbon tetrachloride
MTBE ----Cadmium chlordane --
V pc.,1!:, --Chloride <:0,000/ chlorobenzene ------
Chromium chloroform ------
m
--__ Copper o-cresol --
--Fluoride m-cresol ----Iron p-cresol ------... Lead cresol --
m
----
--__ Manganese --1,4-dichlorobenzene
.. Mercury 1,2-dichloroethane ----Nitrate __ 1,1-dichloroethylene ----
E Selenium 2,4-dinitrotoluene ----
Silver heptachlor ----
Radiochemistry Sulfates hexachlorobenzene ----
D ······-·· Zinc hexachlorobutadiene
Parameter Results (PCi/1) ----
_pH hexachloroethane
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
D --Gross Beta TDS nitrobenzene --TOC __ pentachlorophenol --__ pyridine --
D
Microbiology --__ tetrachloroethylene
__ trichloroethylene
Parameter Results (Col/lOOml)
1
_ __ 2,4,5-trichlorophenol
--__ 2,4,6-trichlorophenol
--I-vinyl chloride --endrin --lindane
~~~ Date Received Reported by --
D __ methoxychlor
/'GB-" q-'!-~7 'P __ toxaphene .
Dale Exlraclcd~\ 1 ·Lf ,'f 1 t::-ll-· Dale Reported 2,4-D
tfiijj-9-s-ffV'P
--
D 973426
_ 2,4,5-TP (Silvcx)
Dale Ana!y1.cd&,i,4 'i.-S::-9.7-A'lJ Lah Number
1)1 !S 319! (Revised 2/91)
--
STATE LABORATORY OF PUBLIC HEALTH
P.O. BOX 28047 -306 N. WILHINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEHICAL ANALYSIS
/NEUTRAL ANO ACID LAB NO q7 -lc//J"I 9'7.-3<1/0 <;73<J/ I '773'11.J.. '?7,-(0, -f
EXTRACT ABLES FIELD# _:7/) ::i O ;:i ~n . , , -"o::tn' '7A,'~n(,, .:Jo:::,,o,
n COHPOUNO TYPE r I l ( ) ( / ) I I > < I l
UNITS .. n/ l )......., v.-:;;;1 "-'""' tun/ l '-"-v; ,n/ l lmfio un/l
N-nitrosodirnethvlamine /()/ ;,/".fA .. IA..-. ;.A--•
b' (2-ch loroethvl )ether
2 hlornohenol ,
n nol . •/
Eichlorobenzene . , JDK
ichlorobenzene JOY ..tu
ichlorobenzene " '18.
bis[2-chloroi=rnnv] )ether •
h ch l oroethane
N itroso-di-n-nrN"'lvlamine
n i trobenzene
~ nhorone
itroohenol
2 -dirnethvlohenol
bis(2-chloroethoxv)rnethane
1-d i ch l orooheno l
4-trichlorobenzene ,,
naohthalene /OK
achlorobutadiene ', -
h l oro-m-creso l
·1.lorocvcl~ntadiene
-trichloroohenol
hloronaohthalene
a naohthvlene
dirnethvl ohthalate
-dinitrotoluene
naohthene
2.4 dinitrnohenol so, '"150
1-dinitrotoluene 10, 3.~()
itroohenol <"Q, i,_-:o
fluorene /0 '~30 , ·h loroohenvl ohenvl ether -
1 •thvl ohthalate _i,
~-dinitro--o-cresol so, 11,, ,n
9i henvlamine /0/330 I ""'nzene
rmnnhenvlohenvlether
hexachlorobenzene ~
tachlornnhenol SOll~S'O
nanthrene //1 /?:Jo
anthracene
utvl ohtha late I I I I . . ' ,I oranthene ,, ' '\
rn1) L
'
Estill\ated value. H,.o/sou ...
Actual value is known to be less than value given.
Actual value is.known to be greater than value given.
U -Haterial was analyzed for but not detected. The nurber
,, -Not analyzed.
is the Hinin>.JTI Detection Limit. mTJL -----Tentative identification. -. On NROC List of Priority Pollutants.
I
CI)
, ·-i·.,,a
Jn '?r, V
r I )
.. n/ l,
t.,(._
~
'\
0
D
E
I
I
I
I
I
I
I
h
I
I
BASE/NEUTRAL ANO ACID
EXTRACT ABLES
CXlMPOONO
nvrene
benzidine
butvl benzvl ohthalate
benz(a)anthracene
chrvsene
3 3-dichlorobenzidine
bis (2-ethvl hexvl l ohtha late
di-n-octvl ohthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(alovrerte
indeno( 1 2 3--cdlnvrene
dibenzo(a,h)anthracene
benzo(o. h i l=rvlene
ani 1 ine
benzoic acid
benzvl alcohol
4--chloroaniline
dibenzofuran
2--rrethvlnaohthaleoe
2--rrethvlohenol
4--rrethyl phenol
2 nitroani line
3-nitroani 1 ine
4-nitroani 1 ine
2 4 5-trichlo=henol
J -Estimated value.
STATE LABORATOOY Of PUBLIC HEAL1H
P.O. IJOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 21611
ORGANIC OlEMICAL ANALYSIS
LAB NO 'f7 ~ , 7/7-?<l//J 073'./J/ I ,...,..f/ _1
FIELD # ::io '.1.cJ =? .;?02 0<1 .:::J03o' ,::;JC)':30L.
TYPE ( ' ) '' l
' I ) < I l
UNITS ' ,,n/1 '\_ ••n/] 'l=~ "n / l ~ ....-,,n/1"\. " I
Jo/~:?o vi--IA-1A \A.-
t'A i,,.so
/0/3.30
.I,
so/1L"O
Jo/330
/0/s~O
.so/J1n,o
r I I /
,.✓ ' ' '
,...o 10-r:-o I,. . • A -lA--IA--
• .,
/() 1=,,
.,,,
s-ot,r.<o
/ ' / I
,/ \. • I ' "
frl])L-
H2.0I Soll-
to be less than value given.
q7.3111 ~
;;;1a307
1 I 1
.. n/lJ ,.
l.,A.._
/
\
I
,
'
JOI<'
LA-
.
\
K -Actual value is known
L -Actual value is known
U -Material was analyzed
NA -Not ,malyzcd.
to be greater than value glven.
for but not detected. The nurrbcr 1s the Hinirrun Detection Limit.
1/ -Tentative identification.
~/ -On NRDC List of Priority PolluLrnts.
Y,, ;,, I
...;)-J~OR
r / l
.. n/j ")-...,
,A
/
'
IA-
/
'
STATE LABORATORY OF PUBLIC HEALTH
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 276 l l
ORGANIC CHEMICAL ANALYSIS
/NEUTRAL AND ACID LAB NO U I~'//\-
EXTRACTABLES FIELD # "'0-'.0'1
TYPE ( _:, ) n COl1POUND ',,n/1).~ UNITS
N-nitrosodimethvlamine tnl 2~"
b. (2 chloroethvl )ether
2 hlornnhenol
n nol
l 3-dichlorobenzene
1-dichlorobenzene
-dichlorobenzene
bis(2-chloroi•nnrnnvl)ether
~ ach l oroethane
itroso-di-n .nrl"V'lvlamine
robenzene
l n.horone
5 itr<Y'lhenol
2 -dimethvlohenol
bis(2-chloroethoxvlmethane
1-dichlo~henol
.. 4-trichlorobenzene
naohthalene
achlorobutadiene
hloro~resol
he hlorocvcl=ntadiene
trichlorf'Y"lhenol
hloronaohthalene
naohthvlene
dimethyl ohthalate
1-dinitrotoluene
n>nhthene
·2.4-dinitrnnhenol SO/lbSO
a-dinitrotoluene IOl.'f~O .
nitrnnhenol .,o/tr,,,;o
uorene /0/~30
ihlornnhenvlohenvlether
thvl ohthalate "' -dinitro--o-cresol so, /1,,'{0
di::,hen'llamine /01330 t !>benzene
,rrn-r,,henvlohenvlether
hexachlorobenzene ,,
ltachlornnhenol so/11,,:ro
nanthrene //l/ 1'?0
hracene
dibutvl ohthalate
oranthene \I
rn 1) L
Estimated value. f{,.o/sou ...
' ,,
I
-, , -t ./ J / __
.JO~iO
( _,. >)
i,';;o/l "
' ,,
I
. Actual value is known to be less than value given.
Gf-✓-< VI 7
::io-;::,,11
/J)
un/i}-.
• A
I
'
'17~(,// 9 _)~ -;;,.;,;z.
/ . .J)
'-',in/ l ). -"'·-,,,
.
/
'
o/7:::f(,/.I'>'
,;2.o ~ I =l
,,;, )
", t~/ 1 '-----
-tA -
/
'
' Actual value is known to be greater than value given.
Material was analyzed for but not detected. The nurrber
NA -Not analyzed.
is the Mini1TU11 Detection Limit. m])L ----I -Tentative identification.
-On NRDC List of Priority Pollutants.
I
4'73VJ/J
;;).0~1u.
/_.,).
.. n;JJ..-
I A
/
'\
I
D
I
I
I
I
I
f
I
I
I
I
I
I
It
I
I
BASE/NEUTRAL ANO AC IO
EXTRACTABLES
COHPOONO
rivrene
benzidine
butvl benzvl ohthalate
benzfa)anthracene
chrvsene
3 3-<Jichlorobenzidine
bis (2-ethvl hex vi l nhtha I ate
di-n-octvl ohthalaie · .
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(alnvrene
indeno( l.2 3-<:dlnvrene
dibenzo(a h)anthracene
benzo(a h i ,~rvlene
aniline
benzolC acid
benzvl alcohol
4-<:h l oroan i l i ne
di benzofuran
2-methvlnaphthdlene
2-methvlohenol
4-methvlohenol
2-nitroani I ine
3-ni troani 1 ine
4-ni troani line
2 4 5 trichlo~henol
J -Estimated value.
STATE LABOAAlOOY Of f'UBL!C HEALlH
P.O. BOX 28047 -306 N. ll!LH!NGlON, 51., RALEIGH, N.C. 21611
ORGANIC QjEHICAL ANALYSIS
LA8 NO a7:tc/1, "7 -1-c::-1~ <-t7-', 'II 7 <-t /3'-II y
FIELO # ..,~ ~o q ·7 ~'.;?I r, .::7 O-'i/ I ,;}_() --.1 ,,)._
TYPE r .-'.> l '~l ( co<) r,,? l
UNITS V' ua/ l ' ,.n/1 '\,...&c. ..n/1 ).=-,< ~all'""""'
Jo/~~o I ,L_... A IA -A..-,
..,.,, ;,,.<o
/0/330
.
.I,
.so/11,.,;o
10/330
/0/.1.::/o soh,.<o
/ I / r
,/ ~ I \ I \ I
..-0 111-""0 ll'--I A_ -I.._ (/\.._.
' ,,
/() 1~11
,1
S'O''u:·o
, , , / ,, . I • I \ ' I
..
mn1-
HzOI Soll.-
to be less thdn value given.
07qv,q
~0-::l.1~
r '7\
un/ I),.,..,._
'
/
\
I
/
'
K -Actual value is known
L -Actual value is known
U -Katcrial was analyzed
NA -Not analyzed.
to be greater than value given.
for but oot detected. The nurt:>er is the Minirrun Detection Limit.
1/ -Tentative identification.
~/ -.On NRDC List of Priority Pollutants.
<J=c/.20
1 ~ ::,_/ti
(..;2_)
un/]\ _;1._
vL-
/
\
(.,<._.
,
' /
STATE LABORATORY OF PUBLIC HEALTH
P.O. BOX 28047 -306 N. ~ILIIINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
/NEUTRAL AND ACID LAB NO a7 .qVJ / I/ ,,.,c'v·-,, YQ=I <-t7 ~Val</ I/..<~""'\
EXTRACTABLES FIELD # •?r,'2,< ?o:J.il--,0 ::i.17 .::7 0 ::? I ,f-' c,2.0~ /'I
COl1POUND TYPE /..;)...) ( /) I I ) ( I ) ( ..;l)
.. .. ,.,;(' ,. ua/ 1 }._ ,1~-.
UNITS .. n/ l ' -,,. -' 110/'"" ,.n/1
N nitrosodirnethvlamine 10/::,;r,. . , .. . , 0 A IA
bis(2-chloroethvllether
ruhlor~henol
nol
1,3-dichlorobenzene
1111-dichlorobenzene
1 ■1-dichlorobenzene
bis (2-ch loroi snnr<vwl )ether
~ achloroethane
i troso-di -n-nroovlami ne
n1 robenzene
is )horone ~ itr~henol
-dirnethvlohenol
bisf2-chloroethoxv1rnethane
-dichloroohenol
I 4-trichlorobenzene .
naohthalene I achlorobutadiene
h l oro-m--creso l
!!_e llorocvcl~ntadiene
2 trichlornohenol ! hlorona□hthalene
naohthvl ene
dirnethvl ohthalate
1-dinitrotoluene
naohthene
2 4-dinitr~henol S0/4foSO
~ -dinitrotoluene 101.~~o
~ itr(V'\henol s-o/JJ,..::o
t orene /0/~30
4-chlor~henvl □henvlether
lthvl ohthalate ,
-dinitro--o-cresol so ~r-<o
diohenvlamine /0/330
nzene -rmoohenvlohenvlether -hexachlorobenzene '\I
I tachlor~henol so/11,,:ro
f ~nanthrene l/1 /~.'JO
2 hracene
dibutvl ohthalate / j I I /
oranthene V \ ' ' f
'\ I
m"])L
Estimated value. H,.o/SOI '-·
Actual value is known to be less than value given.
Actual value is known to be greater than value given.
Material was analyzed for but not detected. The nurber 1s the llininun Detection Limit. m])L ---NA -Not analyzed.
I -Tentative identification. _ -On NRDC List of Priority Pollutants.
I
c;7 =?y,...l /-
.Zc:,3 2r,
( LL l
.. n; I"" . ..
/
'\
D
D
I
I r
I
I
I
I
I
I
I
I
BASE/NEUTRAL ANO ACID
EXTRACT ABLES
aJMPOOND
nvrene
benzidine
butyl benzvl phthalate
benz(a)anthracene
chrvsene
3 3--dichlorobenzidine
bis (2--ethvl hexvl l nhtha late
di n--octvl ohthalate
benzo(b)fluoranthene
benzo{k) fluoranthene
benzo(alovrene
indeno(l 2.3--cd)nvrene
dibenzo(a h)anthracene
benzo(o.h il=rvlene
aniline
benzoic acid
benzvl alcohol
4-ch l oroan i l i ne
dibenzofuran
2-methylnanhthalene
2-methvl Dheno l
4-methvlohenol
2-nltroani 1 ine
3-nitroani line
4-ni troani 1 i ne
2.4 5-trichloroohenol
J -Estirru.ted value.
STATE LABOAATOOY Of f'\JBLIC HEAL1H
P.O. OOX 28047 -306 N. \o/lLMINGTON, SI., RALEIGH, N.C. 27611
ORGANIC O1EMICAL ANALYSIS
LAB NO '-f 7 ,f '/ .J. I 97-<<l.2) '17 ,( '✓-2 ~ <../7'<Y.2. V
FIELD# ~02, i _;io;:}.1/A .)..o:?17 -~ o =<1 Y
TYPE (-' ) ( / l ( / ) r / l
UNITS ., un/ l .. nih ,·~ '"~ rwf/l~ ,10/l ) _ ,1,_
/O/'?'?l'I IA--' . . ,A -
'.-n /,1.<o
/0/330
,I,
so/1t.,;o
10/330
/O/.s.:.o soh,.,o
/ I I I
' / ' ' ' '
<oh1,.ic-o II--I -I A \ ,L__..
~ ,
/0 /~J'I
,,
s-o ,, 1,,50
/ I / / ,, \ \ \ \
fr)])/_
Hz.0/ Soll..
to be less than value given.
<J7-?V,,2 'I
,.;}CJ :;1,/~
r ..,,z l
',,n/1'"'1 ..
I •
/
'
IA--
/
'
K -Actual value is known
L -Actu.31 value is known
U -l'\aterial was analyzed
NA -Not analyzed.
to be greater than value given.
for but not detected. The nlflOer is the Hinirrun Detection Limit.
1/ -Tentative identification.
~/ -On NROC List of Priority Pollutants.
It;.., ~, ... :1/
-:, c;, 3:;;:::
{ ~l
.--;,nj].,_____
(.A__
7
I
(./4.._
/ '7
,' I
· · NCDEHNI~
D . . Division of Waste Management lBI: Superfund Section
□ Hazardous Waste Section ue D Solid Waste Section
Organics Lab: V
lnorganics Lab:~~
D
D
0
E
I
I
I
CHAIN OF CUSTODY RECORD
r
I
I
I
I
I
I
I,
I
I
Project Name: ':::if)_IYl0175 ~·c_ 7Zullc-Sampled By: L)o,1f'A... ()Jr' /.,,o,.
Site ID# (NCD#) Ne.../) oto Z-5~ 7q-z._ Sampler ID
Location: $1a:f-es,,. / / / !_, /\JC Telephone:( 1i't9 ) 7 ~3-7-'?Ju/ qd-3i7 Address: 174'3 CJ-h)/;..__ /2.d. Date Sampled: 9{z.sL11 , eoLu(<11
Time Sampled:
Sample Types: Soil Water (/ Waste Other
Remarks:
'
Field Sample o-?»7-'0"f-07.,.o?-'c,S 62.o'Z.'Cb c::11 .. crz_ 'Q 7 o?J::, q:£3 DZV?_~ c52-<o2'76
Numbers 12-z.-ozq1 tfU:iYfZ--o?o'l-°/ 3, 0 7.Jb<-94 D ?-,,:, '2. "IS ov:,?q~ c?e,2-q7
o7.-o ?Pf '6 O&Ol--Cfr Ow=?,q::i 0 l-0 "?cP/ Qt,C~'2.-
i • ,-;$ .~/ .... ~ h. Relinquished By: /' Date:_1/2/jir7 Time: /yi)
(Sien°«rc1 -~ V ,/) ' -
Received By: v)J/'~;JrJ,.~ (' J-10, IA Date: f ~"i1-R-97 Time:
(Signature) V
Relinquished By: ' Date: Time:
!Sienature)
Received By: Date: Time:
(Signature)
Relinquished By: Date: Time:
fSi1111aturc)
Received By: Date: Time:
/ ,~;S'iature) .
Results Repor~ ~A '-4(•!\...eaY Date: q /,l.3/4'7 Time:
rnturc) · . I I I
1'\'.((: 0~par1n111•1: crE·1,t,:,nmcnt,
: lcal:h, & Natural Rcso.:rr-:s
Solid Hast: Managcincnt D'.vi.'):on
SA}Vf PLE ANALYSIS RE<ftiE©i::JVE:D Stale Laboratory of P,b1;, Health
P.O. Box 28047, 306 N. Wilmington Street
.. SEP 26 1997 Raleigh, North Carolina 27611
.IJA'>ite Number /vc_r_0 :_:..__:s;=--S_:....,:_-:__:7:_0_,._, _2-___ Field Sa;;rnle Number b LOW:-u-~uPERFUND SEC I IOl'f':
. Name of Site S(5rno/l s y:€-kc..-7?!,/t/C.. Site Loca:ion Sides //i / le...
D . Collected lly __ ___,,,...,::S:::'._____ ID# ___ Date Coll~cted __ t3.,_{_7-_w_ . .,_/ q..,_,7'--------Time_,_{ 1--'-"3.'--0 __ _
~ \
Agency: Hazardous Waste Soiid Waste /. _1_Superfwld TCLP Compounds
Sample Type Results(mg/1)
Environmental Comments
Ino11?••ilc Compounds
A:--senic
V Ground water (1;
___ Surface water (2)
__ ~oil'(3)
_ Solid (5) {)fW{ J0/J{1 (.JJe{ (
Barium
Cadmium
Chromium
_ Liquid (6) i--Df'.I /U/C.../ t\J{:;f-W/Jr[f:I?-: Lead
_ Sludge (1) __ t).-f-=--l_l_"rf-_____ _ Mercury
Selenium
I _· O:her (4) _ Other (8)
Sii\'ir
I ,-I -
Organic Chemistry Inorg::nic Ch'.!mistry
11 P,· .. 11:nc!ec Result;(mg/1) , .Parameter
. V l'&T:GC/MS I Arsenic r--A,;,'.:!o/~· fa1. I --Barium
MTBE I = Cadmium
Chloride -------------
' ______ I Chromium -1-
1 ! --;l~1!~;;~;c
Iron
Lead
Rm,::s(mg/;j(m;;/kg'. · Orianlc Compound,
ben~er.e
c&:-u:.::>r. tctracni:)ricic.
ch:ordane -----------
-----·---1 chlorobenzenc
chlorofon,, -------i : ·· · -o·crcso!
rr.-crcso:
-· p·cr:::sol
cresol
Resuits(mg/1)
------
1'1
-· Manganes~ _______ ,. 1,4-dichlorobcnzene
11----------1
I
Radiochemistry
Ii I
h1rameter
__ Grnss Alpha ______ _
Results (l'Ci/1)
Gross Beta 1! 11----------------J
l \
1
____ M_ic_r_o_b_io_Io_gy ____ --J
f'ilriln,eter Results (Col/lOOml)
I
I
I
__ Mercury
t-itrate
Selenium
Silver
Sulfates
Zinc
pH
1,2-dichlorocthane
,
1
__ 1,1-dichloroethylcne _
_______ 2,4•dinitrs>tn!uene ____ _
_______ __ heptachlor _____ _
hcxachlorobenzene
hcxachlorobutadiene
hexschlorocthane ------
__ Conductivity ______ _ __ methyl ctr.yl ketone _____ _
TDS n'.~robenzcne
TOC pentachlorophenol
pyridine
__ tctrachloroethylcne
trichloro_ethylene
__ 2,'+,5-trichlorophenol _____ _
__ 2,4,6-trichlorophenol _____ _
__ vi11yl chloride
cndrin
lindane
D
N.C'. Dcp:lrtnhnl of E:;vironmcnt;
J lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory o( Public Health
P.O. Ilox 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
~ile Number---'M-----"r,C.,i)<---.C.l{;--=...c~--"s'-s_5_7-'----!1_2... ___ Field Sample Number (0 -Z..o'2-'o.S
. . Name of Site_S,,~lj'+m~o~/I_S~~>t?=~-f,_•c..-_~74~~/l~/c... __ Site Lo.cation Sfde;svr //e_ E . Collected By __ ~/l~?..-. ______ ID# ___ Date Collected ca/z.sf q7 Time_~/7~5_"3 __ _
Agency: Hazardous Waste Solid Waste · VSuperfunc!
Sample Type
I Environmental
V Ground water (1)
Concentrate Comments
_ Solid (5)
m __ Surface water (2)
_ S,oil (3)
_ Liquid (6) <f--l)rz_;I\)~ N(:J--
-Sludge (7) Wit Tel?... CUf;{J._,,,,.
m _ Other (4)
,--
Organic Chemistry Inorganir Chemistry I
.
I
t~1-Parameter
VP&T:GC/MS
.• Resulls(mg/1) Parameter,.• Res•Jlts (ml," 11) (mg/l'f.'J
__ Acid:Bji, Ext.
MTBE ·--; ~ --
--
.. --I :-. --I --
·-·, ~:. . --{·\ --
--
Radiochemistry
I
I
I
I
I
I
Ii
I
I
······-··-
i1aramctcr Results (PCi/1)
__ Gross Alpha
Gross Beta --
Microbiology
Parameter Results (Col/lOOml)
--
--
Date Received AUG 2 8 1997 f;;.9
l):;tc Exlraclcu
Dale Analyzed 9-1 5-9'7 -1,j
/)11.S Jl1JI (l~cvi.<;cU 7N1,
Arsenic --B'1ri-Jm --Cadmium --· Chloride --Chromium --__ Copper
Fluoride_ --Iror. --Lead --__ Manganese
__ Mercury
Nitrate --Selenium --Silver --
Sulfates --Zinc --_pH
__ Conductivity
TDS --TOC --
--
--
--
--
--
--
Reported by
Dale Reported
L;ib Number 973428
.
I
i' ;.-
I
I
I
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
--Selenium
Silver
. Organic Compounds
benzene
.-:arbon tetrachiorid:.
chlordane
, chlorobenzene.
• •chlorofo: m--
o-cresol
m•cresol
p-cresol
crcsol
• 1,4-dichlo, obenzcne
1,2-dichloroethane
__ 1,1-dichloroethylene
2,4-dinitrololuenc
heptachlor
hexachlorobenzene
hcxachlorobutadiene
hcxachloroelhane .
Results(mg/1)
Results(mg/1)
-------
-------
------
__ methyl ethyl ketone _____ _
nitrobcnzene
__ pcnlachlorophcnol
__ pyridine
__ tetrachloroethylcne
trichloroclhyiene
__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol
--vinyl chloride
endrin
lindane
methoxychlor
toxaphcne
2,4-D
2,4,5-TP (Silvex)
------
------
N.C DcpartnH,nt of Er,,ironmcnt,
I lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST Stale Laboratory vf Public Health
P.O. Box 28047, 306 N. Wilmington ~lrcet
Raleigh, North Carolina 27611
~~ilc Number A/~O .ct?~ SSS 71 Z... Fielc! Sample Number bl.0""2-~(,
Name of Site S.,3rno// S ';::q?-kc__. 7a,;t/c.. Site Location Sfde,r //1 / /e___
.E Collected By st-ID# ___ Date Collected ~/zs/ 1, Time 1712
E Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds
Sample Type
I Environmental Concentrate
.. V Ground water (1) _ Solid (5)
Comments
Inorgan;c Compou11<ls
Arsenic
Barium
Cadmium
Chromium
m _· _ Surface water (2) _ Liquid (6) Lead
_ Soil (3) _ Sludge (7)
Mercury
Sclen:um
Silver I _ Other (4) _ Other (8)
Organic Chemistry
►· • ·' l'urnmcter ; 1 v., P&T:GC/MS .~ .t• = Acid:B/N Ext.
',· . _MTBE
;, -·-___ . ___ ------
Results(mg/1)
!
1: I
Inorganic Chemistry ·
Parameter· .. · Re,ults(mg/l)(mg/lG!) I
Arsenic
Barium
Cadmium
Chloride
Chromiun:
__ Copper
Fluoride
Iror.
Lead
0~.Rnic Compo11m1s ·
be:11.cne
. carbon tctrachk,.:Ce
_. __ .<;h!ordanc
cr.iorobenzcnc
_______ 1 __ chloror?"'"
O•creso.
m-cresol -------1 __ P·creso~
Results(mg/1)
Results(mg/11
I' __ Manganese
__ Mercury
Nitrate
Selenium
Silver
Sulfates
Zinc
-------j' cresol _______ · __ I,4-d1chiorobcnze11c. _
lr--------l
Radiochemistry
I .Paramder Results (PCi/1)
__ Gross Alpha ______ _
pH
Gross Bela I !~---------I
I Microbiology
__ Conductivity
TDS
TOC
1,-P_a_r,-.,,-,c--l-,r ___ R_c_·s_u_lt_s_(_C_o_l/_l_OO_m_l)~
I
I
I
AUG 2 8 '\!197 bD Date Received Reported l,y ------------------
Dale Extracted ________ Dale Reported ________ _
Date Analy1.cd 9-16-91 "f)j
1)1 IS J1 1JI (llcvi.~cd ?N1'
Lab Number ----------973429
1,2-d ichlorocthano
1,1-dichloroethvlene
:,4-dinil rotoluene
__ heplachlor
hcxachlorobenzene
hexach,orohut adiene
------
hexachloroelhane ------
--:,ie'.hy! ethyl ketone
nitrobcn1..cnc
penlachlorophcnol
pyridine
__ tclrachloroethylene
__ trichlorocthyic1,~
__ 2,4,5-trichloropl:enol
__ 2,4,6-trichloropheno!
vinyl chloride
cndrin
lindane
mclhoxychlor
loxaphcne
2,4-D
2,4,5-TP (Silvcx)
------
------
N.C.' Oep::inmc,11 of E1Jrironmen1,
1 lcalth, &. Natural Resources
Solid \.v'aste Management Division
SAMPLE ANALYSIS REQUEST State L.aborntory of Public Health
P.O. l3ox 2S047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
.-~ite Number-'M-=[,:..Q'--=0;;--""---Z....=--=S=-S-=5'----'-7-'C/'-2... ___ Field Sample Number b W '2-i 7
. . Name of Sile Si.3rno// .5 Sy?n'c... Ya,1,./c.. . Sile Location Sfd-es Vi '(/e_
. D Collected By JS. ID# ___ Date Collected '6/.rz-to{q7 Time_~t~·D_3_J' __
D
n
D
D
Agency: Hazardous Waste Solid Waste VSuperfund
Sample Type
Environmental Concentrate Comments
V Ground water (1) _ Solid (5) Poff!, UJf (/
_·_Surface water (2) _ Liquid (6) '\(J-Df!{N /c//lf{j-
-Soil (3) _ Sludge (7) /)I\-7£-Y<._ · IJJ6(_j,,"'"'
_·_ Other·(4) Other (8) SS---o,4--pw I
Inorga,1ic C.hemistl)· 1
1-------------1-------------
(' ll ! htrame!er . . ResuHs(mg/1) Parameter Results(m~/l)(mg/ki;) IJ · L,....-P&T:GC/MS Arsenic
•.• , ~ -~~~.!/N Ext. ------1 ~;~o;Tut
Organic Chemistry
I j ______ Chromium
__ Copper I: Fluoride
. / Iron
Lead 11 ·;,, __ Manganese IJ .::,,.· __ Mercury
m 1---------J
Radiochemistry
Nitrate
Selenium
Silver
Sulfates
m Parauu~tu_
Zinc
Results (PCi/1) __ pH
__ Gross Alpha ______ _ m I· Gross Bela
__ Conductivity ______ _
TDS
TOC
Microbiology
Par.ir:1clcr Results (Col/lOOml)
Onie Received 'AUG 2 8 1!197 f3A} Reported by ________ _
Date Extracte<l ________ Dale Reported _______ _
Dale Analy1.cd q-[/5-C/7 nJ Lab Number 973430
IHI..: "ll!/1 /11,-,,;,.,.,l 'J/01\
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium
Chromium
Lead
__ Mercury
Selenium
Silver
Orgttnic Co111po11nuc.
benzene
carbon tclrach;ori<lr.
cHordanr,
cliloroDenzene
ch!orofor;,_
o-cre~o.1
m-creso:
p-·creso1
cresol
1,4-dichlor obcnzene
__ :,2-dichlorocti.ane
Resuils(mg/1)
Results(mg/1)
__ l,l-d1chloroethylene _____ _
2,4-dinitrotoluene
__ heptachlor
hcxachlorobenzene
hexach lorobutacliene ------hexach!oroclhane
__ methyl ethyl ketone ______ _
nitrobcnzcne
__ pcntachlorophenol
__ pyridine
tctrachloroethylene
trichloroetl1ylene
_ 2,4,5-tric!ilorophenol _____ _
__ 2,4,6-trichlorophenol _____ _
__ vi .. yl chloride
c:idrin ·
lindanc
mcthoxychlor
toxaphene
2,4-D
_ 2,4,5-TP (Silvcx)
N.C: Ocpartmont of Environment,
I lea Ith, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST Stale Laboratory of Public Health
P.O. I3ox 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
,~ile Number--'M-=Cc..O'--.G0-=-2-__ s_S_5_...:.7-'C/'--2... ___ Field Sample Number D "°2...€:, -z.__ ca~
. . . . Name of Si_te_· _St~&.c.,'. ~rn_o~/1_.S_~Y'f~-n_'c.... __ ffi~~;t_/c~c. __ Site Location Sf d-e,s /// '( le..
E . Collected By /'\ z_. ID# ___ Date Collected ea/,z&, /q 1 Time __ (_7_2~•8 __
Vs u pe rfun d '
E Agency: Hazardous Waste. Solid Waste TCLP Compounds ----
Sample Type Resulls(mg/1) Inorganic Compouncis
I Envirorimental Concentrate Comments Arsenic --
(}'\.()(\ (-ki( {,{}e! I Barium
V Ground water (1) --Cadmium _ Solid (5) --
IYlS1)z. Chromium I --__ Surface water·(2) _ Liquid (6) Leaci --_ Mercury
_ Soil (3) _ Sludge (7) S,S.-OS-6-W -Selenium
I --Silver
_ Other _(4) --_ Other (8) --
' --Ii I --Organic Chemistry Inorganic Chem:stry r ----------
I · Pnramcter · Results(mg/1) Parameter Results(mg/l)(mg/kg) Organii: Compounds Results(mg/1)
VP&T:GC/MS Arsenic bt:nZ~tJe --l -·
~·-Acid:ll/N Ext. Barium car~iori tctrach:c,ri0· · --I --MTBE Cadmium I chiordane --. ----
Chloride l chlorobenzene ----Chrorniu11. chioroform -------
II --__ Cop;,er o-cre~o ----Fluoride m-crcso, .,,. ----Iron __ p-cresol ------II --., Lead c:-eEol ----
--~.-,·_ Manganese 1,4-dichlnrobenzcne --·---
--·'· __ Mercury 1,2-dichloroethane --Nitrate __ r,1-dichloroethylene ..
·---I Selenium ·2,4-dinitrotoluene --Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene --' --I ""••·-·· Zinc I hexach lorobutadiene ---· 1~aramctcr Results (PCi/1) pH I hexachloroethane ----__ Gross Alpha __ Conductivity __ me:hyl ethyl ketone
I Gross Beta TDS nitrobenzene ------TOC __ pentachloropheno: --
--__ pyridine
I Microbiology --__ let,achloroethylene
. __ trichloroelhylene --Pararnt:kr Results (Col/lOOml) __ 2,4,5-trichlorophenol . --
----__ 2,4,6'trichlorophenol
--vinyl chloride ----endrin · --
AUG 2 8 tl!J7 f!f) Re~orted by
lindane
I Date Received --
--melhoxychlor
toxaphcne
Dale Extracted --Dale Reported 2,4-D --
I 973431 _ 2,4,5-TP (Silvex)
Date Analyzed 9-15-91 -nj Lab Number I l\1 I\.' 'IH\I Ill-. : .... A "'I Int\ --
N.C. Oepartm!..nl o( E,wironmcnt,
l lcalth, & Natural Resources
Solid 'waste Management Division
SAMPLE ANALYSIS REQUEST State l...aboratcry of Public Health
P.O. Box ~i, 306 N. Wilmington Street
Raleigh, North Carolina 27611
~Sile Number-'M-----"'r,"',o'---"_~-=-"~--"s;_S_5 __ 7__,_1_Z.. __ ~ Field Sample Number ___ _,,Q""-c.,=c:o=--Z:--"9f}..::. +------
. Name of Site_y.,_IJ=.:.rn.:.:oc:.:/1..:.=:S:__=Yf='---f,_•..::c...:____,ffi~"-/-'"1./<'-c.__ Site Location _ _,S>-Li~¼"'--'""--'~'--'/C..'Lc//2ece_.=----------
D Collected By __ _,.J=·~s='-----ID# ___ Date Collected __ 'v__,/c..'¾_,_( q_l.,__ __ Timc __ /_3_,/c..6 __ _
D Agency: Ha,.ardous Waste Solid Waste Vsuperfund TCLP Cor.:pounds ----
Sample Type Inorganic Compounds Results(mg/!)
Environmental Concentrate Comments Arsenic --
· VG round waler (1) u.,e ll Barium
Vvt.bl\J w r --_ Solid (5) Cadmium --
E ~£5,~t;e ~ b,V1l~ Ch1omium --__ Surface water (2) _ Liquid (6) Lead --
s S.-v 8.,. C.-w __ Mercury
_Soil (3) _ Sludge (7) Sr.lenium --;)ilver • --_ Other (4) _ Other (8) --,. --r
i ' .
Or_ganic Chemistry --Inorganic Chemistry --,~ I ~\•rametcr Results(mg/1) Parameter Results(mg/i)(mg/kg) Organic Compounus RLst•lts (rng/1)
. •~ P&T:GC/MS Arsenic benzeue ----___ Acid:Il/N Ext. Barium carb0n ktracr.:vr:oe ----
I MTBE Cadmium ch!r,rciane ------
I --.. Chloride chi0;-obenze11c ' ----
I --Chromium chloroform ----
--Copper 0-C!'CSOl I ----
I Fluoride m-crcsol --
'
; ----_,
; --"· Iron __ p-cresol --
" --Lead cresol ----
1. 'iii' __ Manganese 1,4-dichlorobenzcne --~ '.: ... ~· ' __ Mercury 1,2-dichlorocthane -----
' --Nitrate __ 1,1-dichloroethylene --Selenium --2,4,dinitrotoluene
Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene
:1a:-umelcr ----I Results (l'Ci/1) pH hexachloroetha~e ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone
--Gross Bela TDS nitrobenzenc I ----TOC __ pentachloropher,ol
I --
I ----pyridine
I Microbiology tetrachloroethylene --_· _ trichloroelhylenc
P;,ramckr Results (Col/lOOml) __ 2,4,5-trichlorophenol
--__ 2,4,6-lrichlorophenol
--__ vinyl chloride --endrin --. 6{) lindane --D<1tc Received AUG 2 8 1197 Reported by mel hoxychlor --toxaphcnc . --Dale ExlracleJ Dale Reported 2,4-D 9',3432 --
9-l(o-q, _ 2,4,5-TP (Silvcx)
Dale Analyzed -n~ Lab Number -' 1)11<.: 1.llll /!),.,,,,,.,l 1/111'
N.C.' Ocp:1r1mu~t of Er.r,ifOnment,
1 lcallh, & Natural Resources
·~otid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Hcal1h
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
.1f9'ilc Numbcr--'M--'-"C""O"--'C0'-"--=z._'---=s'--S_5_7.c_,1:__Z... ___ Field Sample Number O ~o 210
. Name of Sile~y.....,_!J"'' c;_m.:.,Oe.:/1__:..=S:__=Yf==-n-'-=c...=-_.fat'-="-/t~/,'-c..__ Site Location Sf des Vi l J e....
D Collected By -.,} S, ID# ___ Date Collected (2:,( 2.3{ t/7 Time_._/-'S'-'/c:='..5:__ __
D Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds -- --
Sample Type Inorganic Compounds Resulls(mg/1)
m
Environmental Concentrate Comments Arsenic --
&/oi,JJ Barium
Pf& --__ Ground water (1) _ Solid (5) Cadmium --• p-e., €,I\ fl 1,-_/ ~+,--e:{,/V\
Chromium V Surface water (2) --_Liquid (6) Lead --ss-o,-5VJ --Mercury
Soil (3) _ Sludge (7) Selenium
I .--.,,,.._ --Silver
_ Othc?(4) --_ Other (8) --
--I ;-. -.. Orgnnic Chemistry --Inorganic Chemist~ --: If Pnr:rn1cter . Resul:s(mg/1) Parameter Results (rng/1) (mg/kg) Organic Compounds Resulis(mg/i)
. · V P&T:GC/MS Arsenic be:izene ----··ri-Acid:B/t,; Ext. Barium carLon tctrachlc,ride ----MTBE Cadmium. chlordane 1= .. ' --Chloride chlorobenzcnc ----Chromium ch!oroform I ------. Cop~er o-crcsol I; --------. Fluoride m-crcsol ----Iron p-crcsol
1[
------~•·"'; Lead crcsol --,,: ------I~./·. __ Manganese 1,4-dichlorobcnzcnc ----· --·:,t~·: __ Mercury 1,2-dichlorocthane
--.. Nitrate __ 1,1-dichlorocthylene --I Selenium 2,4-dinitrotoluenc -----Silver hep'.achlor ----Radiochemistry Sulfates hexachlorobenzene ----I ..... ·-··-Zinc hcxachlorobutadiene
Pam meter Results (PCi/1) ----pH hcxachloroethanc ----__ Gross Alpha __ Conductivity __ r.1ethyt ethyl ketone
11 Gross Beta TDS nitrobenzcne ------TOC __ pentachlorophenol --.r --pyridine --Microbiology --__ tctrachloroethylene
·--__ trichlornethylene
I
Par:1mcter Results (Col/lOOml) __ 2,4,5-trichlorophenol i-= __ 2,4,6-trichlorophenol --
--j---vinyl chloride
endrin · --
Dale Received ·1,uG 2 8 11!1e& lindanc
I --Reported by --methoxychlor
toxaphenc --D:ilc Extracted Dale Reported 2,4-0 --I Dale Analyzed 9 -I t,, -qt 11.i 973433 2,4,5-TP (Silvcx)
Lab Number
' ' ' Dll-"iilllf!tn,<.:C'd /ll) -
N.C.' Ocpartmc.'nt of En'.-ironmcnt, · D, .· I lea Ith, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611·
. oe,ilc Number NCO C0 z.. sss 71 z... Field Sample Number __ b_-Z_,.()_-Z__,tf_,( ______ --'--
. Name of Sile Si3rno//S Scp7)'c__ ffi/l/c_ Site Locatio_n Sfq}eyvr '/Je....
D Collected By JS ID# ___ Dale Collected eo/,zs(q-1 Time I W6
D Agency: ---Hazardous Waste Solid Waste --Vs u per fund TCLP Compounds
Sample Type Inorganic Compounds Results(rng/1)
E Environmental Concentrate Comments Arsenic --wru~l Barium --__ Ground water (1) _ Solid (5) Cadmium --
I Chromium
V Surface water (2) --_ Liquid (6) f?lX\ . Lead --
--Mercury
_ Soil (3) _ Sludge (1) S S-o '6 -s.,,,u Selenium I --Silver . __ Other' (4) --_ Other (8) --
I .. --
--Organic Chemistry l:iorganic Chemistry --
I . Parameter . Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results (mg/I)
V' P&T:GC/MS A_rseillc benzcn~ ----Acid:B/N Ex1. Barium carbon tetrachloride ---1.1TBE Cadmium chlordane ------Ch,oride chlorobenzene --------Chromium chloroforrr. ----
I --Copper o-cresoi ----
--Fluoride m-cresol --
I
--Iron p-crcsol --------i.ead crcsol I ----
--I''' __ Manganese 1,4-dichlorobenzene --. __ Mercury 1,2-dichloroethane ------Nitrate __ 1,1-dichloroethylene
I --Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene
I ----.. ,._,. Zinc hexachlorobutadiene
Paramekr Results (PCi/1) ----pH hexachloroelhane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
I Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol --
----pyridine
I Microbiology --__ tetrachloroethylene
--__ trichloroelhylene
Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrir. ---rm efa-lindane I Dale Received AUG 2 8 --Reported by methoxychlor -__ loxaphenc
Dale Extr;;clcd Dctc Reported 2,4-0 --I 9-1 <o-q 7 -rid 973434 __ 2,4,5-TP (Sil·,cx)
Date Analyzed La'.) Number -
-D
.J\'.C.'Dcp.irtmc,.,( of Environment,
,I lea Ith, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST Slate Laboratory of Public Hcallh
P.O. Box 28047, 306 N. Wilmington Street
RBleigh, North Carolina 27611
\ na,ite Number NCO Cr;; 2--SS.5 71 L Field Sample Number ____ b_7o __ '2c~1_L--______ _
u-"Name of Sit_e SJ3rno/l S Syzkc___ 7?!,llfc_ Site Location_~S~i_¼~~V,~r_/~/2~e_~---------
D Collected By j.S, ID# ___ Date Collected __ '6~/_'2._S._{~q_1 ____ Time __ /_3-'-/,-=('.) __ _
D Agency: Hazardous Waste
Sample Type
Solid Waste Vsuperfund
Environmental Concentrate Comments
_Groundwater (1) _ Solid (5) Bac.kcg-ruck\ ,l_
I VSurface water (2) _ Liquid (6) ~,f-P-'e"-r-""e"-'r1"-1t'-/-'--1A"'-/--=s*'-'-----&A--'-~-'-
_ Soil(~)
I _·_ Othe{;(~)
-Sludge (7) --~ss--_-_m~· ~-~S~vJ __ _
Other (8) __________ _
Organic Chemistry Inorganic Chem,stry
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium
Chromium
Lea<l
Mercury
Selenium
Silver
Results(mg/1\
. Puramcter . v P&T:GC/MS
Acid:B/N Ext.
MTBE
Results(mg/1) Parameter
Arsenic
Results(n,g/l)(mg/1.g) ] Organic Compuunds
benzene
Results(mg,'i)
I
I
I
Barium
Cad1nium
Chloride
Chromium -----------·---
.t·
)'{:/'.
J\ 1
•.~-..r
Radiochemistry
Copper
Fluoride
Iror.
Lead
Manganese
Mercury
--Nitrate
Selenium
Silver
Sulfates
I Zinc
Parameter Results (PCi/1) __ pH
__ Gross Alpha __ Conductivity ______ _
I Gross Beta TDS
TOC ---~ Microbiology
I Parameter Results (Col/lOOml)
I Dale Received AUB 2 8 1997 efJ Reported by ________ _
Dale ExlraclcJ ________ Dale Reporlcd_~~~~---
1 9 973435 Dale Analy,.ed -/ /p-q/ -r/j Lab Number
l)IJS 11 1)1 f!tcvi;:ed J/!JJ'\ ----------
carbon lclrachlorid~
chlordane
chlorobenzene
chloroform
o-cresol
m-c1csol
p-cresol
crcsol
1,4-dichlorobcnzene
--1,2-dichlorocthane
------
------
__ 1,1-dichloroethylene _____ _
2,4-dinitrotoluene
__ heplachlor
hexachlorobenzene
hexachlorobut adiene
hcxachloroethane
methyl ethyl ketone
nitrobenzcne
__ pentachlorophenol
__ pyridioc
tetrachloroethylene
trichloroethylene
------
_ 2,4,5-triclilorophenol _____ _
__ 2,4,6-trichlorophenol
--vinyl chloride
endrin ·
lindanc
mcthoxychlor
toxaphcnc
2,4-D
2,4,5-TP (Silvcx)
------
0 N.C. Dcpannu.nt of Er:vironmcnt,
I lea 1th, & Natural Resources
Solid ·waslc. Management Division
SAMPLE ANALYSIS REQUEST State l...abon1ory of Puh!ic Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
~Site Number-'M---'---=[,:..0<-.::~'--"'--=z__'---=s;:....S_5_:.___7..:._!1_Z...___ Field Sam pie Number __ __;o::::_·u.::,=--=:....'2,__:,:fe.c3""-----------
Name of Sile Stjtn0/1 S Syzkc... 7?!,/l./C.. Site Location_....,S..,__fqfey---'--"'•,._·_,_~_,_r'-'-/_,_/2"'e_"'----------
D ~, 11• t:a('Zii>(l}c,.. QO'J.---. . Collected By I..Jt V\ ID# ____ Dale Collected __ -'-----'----'''--'-''----Time ___ u_.c-u __ _
D
D
E
D
I!
Agency: Hazardous Waste Solid Waste VSuperfund --
Sample Type
Environmental Concentrate Comments
__ Ground water (1) _ Solid (5)
V Surface water (2) _ Liquid (6) Jo-SW
_ Soil (3.) _ Sludge (7)
_ Oth~((4) _. _ Other (8)
Organic Chemistry Inorganic Chcroistry
Parameter
VP&T:GC/MS
Acid:B/N Ext.
MTBE
Results(mg/1) l'arameter
Arsellic
Results(mg/1) (mg/kg)
Ba:iw,. --,
Cadmium
Chloride
Chromium
__ Co::,per
Fluoride
· Iron
Lead
__ Manganese. ______ _
__ Mercury
Nitrate E f------------1
Selenium
Silver
Radiochemistry Sulfates
Zinc
Parameter Results (PCi/1) pH
__ Gross Alpha _________ Conductivity ______ _
E Gross Bela TDS
TOC
f------------1
Microbiology ., ___ _
Parameter Results (Col/lOOml)
I Date Received AUG 2 8 1997 fP Reported by
Dole Extracted Dale Reported
I Dale Analy1.ed q-ll.P-97-rJd Lab Number
l)!J...; 11')1 (lirvi~rd ?/()1'
973436
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
Ocganlc Compounds
benzen~
.::arbo,: tetrachloride
chlorC.:e1.nc
cP.lorobenzenc
chloroform
O·CfCSO!
m-crcsol
p-creso~
cresol
1, •.-dicl:lorobenzene
. 1,2-dichlorocthane
Results(mg/1}
Results(mg/1)
------
------
__ 1,1-dichloroethylene _____ _
__ 2,tt-dinitrotoluene
__ heptachlor
hexachlorobenr.ene
hexachlorobutadiene
hcxach!oroethane
methyl ethyl ketone
nitrobcn1..ene
_· _ pentachlorophenol
__ · pyridine
__ tetrachloroethylene
__ trichloroethylene
------
------
__ 2,4,5-trichlorophenol _____ _
__ 2,4,6-trichlorophenol _____ _
__ vinyl chloride
endrin
lindane
melhoxychlor
loxaphcnc
2,4-D
_ 2,4,5-TP (Silvcx)
0 N.C: Dcp.:irtm~nt o{ E1:vironmcnt,
l lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State L.aborntory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Ralcipl, North Carolina 27611
-~Sile Number-"'M__,,cc.ro"-'_.G0--=_;;_.~ _ _;;_s;_S_5_7..;__:C/_Z... ___ Field Sample Number 0--z....t, 2q4
. . _Na1:1e of Site_y_. ~>j""m~o~/1_S~~>J'~~f,_•c.._~ffi~~/l~ft_C.._ .Site Location SfciJes Vi/ /e__
D ., Collected By l) /v'\ ID# ___ Date Collected Co/-Z.0 { t/ 7 Time O'i3 Zo
D Agency: Hazardous Waste. Solid Waste Vsuperfund
Sample Type
m
Environmental Concentrate
__ Groundwater (1) _Solid (5)
Comments
I // Surf ace water (2) Liquid (6) --.
m
_ Soil (3) _ Sludge(?)
_ Othet(4) _ Other (8) . .~
1· -
Organic Chemistry Inorganic Chemistry i
I Parameter · Results(mg/1) Parameter. Results(mg/1) (mg/ki;)
VP&T:GC/MS Arsenic i ';..,,, _ Acid:B/N Ext. --
' Bariun1 I --MTBE • Cadmium ----I --Chloride --Chromium ----
I --__ Copper I
--Fluoride --• ~\ l,. Iron '1 ----
I' --.. Lead ----1\~-: __ Manganese
;·'{ ... ~: __ Mercury --
; Nitrate ----I Selenium --Silver --Radiochemistry --Sulfates
I ······-·· Zinc
Pai:.irnckr --Results (l'Ci/1) _pH
__ Gross. Alpha __ Conductivity I I Gross Beta TDS ----TOC I --
--
I Microbiology --
--~ ,,,, . '""" Results (Col/lOOml) --
--
--
I Dale Received AUG 2 8 f1R f3l2 Reported by
Dale Extracie<l Dale Reporled
I Dale Analyzed 9-17-C/7-n-d Lab Number 973437
l)!IS 1!1JI (llcvi~r:.d ?/l/1\
TCLP Compounds
Inorganic Compounds
Ars~nic
Barium
Cadmium
Chromium
Lead·
Mercury
--Selenium
Silver
O, &dnlc Comp~unrls
b~nz.cnc
i:ar~on tetrad1!orici;,,
ch1orGane
chlorobenzene
chloroform
o-crcsol
m-crcsol
p-crcsoi
cres0l
1 ,t-d:ch1orobcnzcnr,
Results(mg/1)
Rr,sults(mg/1)
------
--------1,2-dicllloroeti,ane ______ _
__ 1,1-dichloroethyleP•.'·
2,4-dinitrololuenc
heptachlor
hcxachlorobenzenc
hex a ch Io rob II I.ad icne
h~:-:achloroetlrnne --; __ methyl ethyl ketone
nitrobcnzenc
r·cntachlorophenol
pyridine
__ tetrachlorocthylene
__ lrichlorocthylcne
_._2,4,5-trichlorophenol
__ 2,4,6-lrichlorophenol
vinyl chloride
cnd:-in ·
lindanc
mcthoxychlor
toxaphcnc
2,4-D
_ 2,4,5-TP (Silvcx)
------
------
N.C.' Ocp::irtmc,nt of Er.,tironment,
1 lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
-oe~iteNumber NCO l{;Z-s-S.5 712... Field Sample Number QL-OLC/5
,, . Name of Site S(yrno//S Sy2·kc..-7a,/l/C. Site Location Sfgfeyn//e...
0. Collected By wM ID# ___ Datc Collected <o(z.s( ,q7 Time __ (_'O_{_S' __
n Agency: Hazardous Waste Solid Waste Vs u per fund
Sample Type
I Environmental Concentrate Comments
· · __ G ro_und water (1) _Solid (5) la1 · s-frett.fYI l.)Je..c +-
m · V Surface water (2) _ Liquid (6) cf si-k
Soil (3) -.. --~-_Sludge (7) SS.-l&,,.,..s,_VJ
I ___ · _ OtheG(4) _ Other (8)
I :-O;ganic Chemistry Inorganic Chem-:stry
:"'·I· 1. Pnrnmcter · Results(mg/1) Parameter
ii,. v"'. P&T:GC/MS Arsenic
/: ~ Acid:B/N Ext. ' --B~riu-;,,
Resul:s(mg/1) (mg/kg)·
, --
C:· MTBE Cadmium
I
I
I t----------1
Radiochemistry
I Parameter Results (PCi/1)
__ Gross Alpha
Gross Beta -------
• t-'---~---1
Microbiology 1,------j
Parameter Results (Col/lOOml)
Chloride
Chromium·
Copper
Fluoride
Iron
Lead
__ Manganese
_·_Mercury
Nitrate
Selenium
Silver
Sulfates
Zinc
pH
__ Conductivity
TDS -------
TOC
I Date RcccivcdAUG 2 8 1997_ [3fl. Reported by ----------
D"tc Extractcu Date Reported
I -----~9=7=3~4~3-8--
Datc Analy,cd 9-/]-C/7,1.J Lab Number
1)11.'-; 11'JI rn.cvi.~t:d ?/!l1, ----------
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium
Chromium
Leacl
Mercury
Selenium
Silver
Resulls(mg/1)
Organic Compounds Results(m!;_il;
be111.ene
carbon tctr.:i.chlori':!~
chlorciar.e
c:'iiorobenzcne
chloroform
o-cresol
;n-crcso!
__ ;.--crcsol
creso!
1,4-dic!ilorobcnzenc
--1,2-dichlorocthane
-------
------
__ 1,1-dichlorocthylen,; _____ _
2,4-dinitrotoluene
heptachlor
hexachlorobenzene
hcxachlorobutadiene
hexachloroethane ------
--methyl ethyl ketone
nitrobenzene
__ pentachlorophenol
__ pyridine
__ tetrachloroethylene
trichlorocthylene
· __ 2,4,5-trichlorophenol ------__ 2,4,6-trichlorophenol _____ _
vinyl chloride
endrin ·
lindanc
methoxychlor
__ toxaphcnc
2,ii-D
__ 2,4,5-TP (Silvcx)
N.c: Ocp.irtmcnt of Environment,
l lcalth, & Natural Resources
Solid Waslc Management Division
SAMPLE ANALYSIS REQUEST Stale Laboratory of Public Health
P.O. Box 28047, 306 N. Wilrr.ington Street
Raleigh, North Carolina 27611
Field Sample Number ___ 0'--7.-D __ .. _z __ Cf'--~"-· ______ _ . oe~itc Number....:A/i-=(;::,0:....=:.~-""--=z_=---=E;=-S-=5=---=7_'J,__2... __ _
. _ Name of Site Starno,1 S y17·kc:... ffi/t/c_ Site Location Sfcde.s n / /e_ . _ _,_J.e:===~==,-==:...c:::._cL.,=.::.!...-=---. D . Collected By J S ID# ___ Date Collected Co [?.S / q 7 Time /72..S ------
D Agency: Hazardous Waste Solid Waste VSuperfund
Sample Type
E Environmental Concentrate Comments
-. _ Ground water (1) _ Solid (5)
I V Surface water (2) _ Liquid (6)
I
_ Soil (3) _Sludge (7) . ' .
.'J
_ Othe°r,.(4) Other (8)
I: I Organic Chemistry Inorganic Chemistry
,---------------1---------------
~r~ 11 l'nri,met:r . · l. . VP& ~:GC/J.1S
!1_~_';,'~;' Ac:d:B/N Ext. 1· MTBE ,.. --.
.. ---------------
Results(mg/1)
i
Ii
•i
Parameter
A1 senic
Ba:ium
Cadmium
Chloride
--Chromium
__ Copper
Fluoride
Iron
Lead
Results (mg/l)(mg/kg)
11---' -----l
__ Manganese
__ Mercury
Nitrate
Selenium
Silver
Sulfates
Zinc
Radiochemistry
I Paramctu Results (l'Ci/1)
__ Gross Alpha ______ _
I f---G-' r_o_s_s _B_e_t_a _______ _
I 1 :. ____ M_i_c_r_ob_i_o_Io_gy ____ _
1 i Parameter Results (Col/lOOml)
pH
Conductivity
TDS
TOC
-------
I Dale Received AUG 2 8 1997 .eJ) Reposted by
D"te Extracted Dale Reported
I Dale Analy1.cd q-11-C/111d. 973439
Lab Number
1111-.: 11111 111 ... _,;~,,,t 1/01\
l
TCLP Compourids
Inorganic Compounds Results(mg/1)
A:senic --Barium --Cadmium --Chromium --Lead --Mercury
--Selenium --Silver --
--
--
---
--·--
Organic Compounds Results(mg/1)
benzene --crirbon tctrachloril1·: --chlordane --chlorobenzenc --chlorofor, . --o-cresol --m-cresol --
--p-cresol
crcsol --1,4-dichlor obcnzc11c --1,2-dichloroethanc --__ 1,1-dichloroethylene ________
2,4-dinitrotolucnc --__ heptachlo:
hexachlorobenzene --hexachlorohutadiene --hexachloroethane --__ me:hyl ethyi ketone
nitrobenzene --__ pentachlorophenoi
__ pyridine
__ tctrac!1loroethylcne
__ trichloroe.thylene
__ 2,4,5-tnchlor,)phenol _____ _
__ 2,4,6-tricWorophenol _____ _
__ vinyl chloride
endrin ·
lindanc
methoxychlor
toxaphene
2,4-D
_ 2,4,5-TP (Silvcx)
N.C.' Ocp:ir1nwnt of Environment,
l lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST Stale Labor:itory of Public Health
P.O. Dax 28047, 306 N. Wilmincton Street
Raleigh, North Carolina 27611
Field Sample Number 0?-o ?....q7 -------~---------ge~ite Number_M--=c~o'-_-~-=-z.. __ s_S_5 __ 7-'1_Z... __ _
_ Name of Site_S,i_,_y"'J' '-m-'-'o"-'//--=.5'----_~Xj7=-:....-f, __ '-=c...=--~M'--"-'-"-/!-'-/,'-c. __ Site Location Sfq,.fcy 1// //e...
_ 0 Collected By frl l---ID# ___ Dale Collected ta(z_s { "f7
0 Agency: Hazardous Waste. Solid Waste Vsuperfund
Sample Type
Environmental Concentrate Comments
V Ground water (1) _ Solid (5) s,;_q/Y\CA.5 U-Jel/
_ Surface water (2) Liquid (6) ~t-/ N ~ /vb-·
_ Soil (~) _ Sludge (7) UJfffe(L Wf(L is
_ Othe~(4) _ Other (8) S.S.-3-z..-pw
I Organic Chemistry Inorganic Chemistry -
,I P1-1rn;ne:cr Results(mg/1) Parameter Results(mg/l)(mg/kg)
1
VP&T:GC/MS Arsenic
·-Acid:B/N Ext.
--Barium --MTBE Cadmium --'' Chloride. ----Chromium -----Copper ;. -----Fluoride
I
--' " --
l~.' Iron I --·, --,. Lead ----
--ti __ Manganese
--. __ Mercury
Nitrate ----I Selenium --Silver --Radiochemistry --Sulfates
I ...... -.. Zinc --Parameter · Results (PCi/1) _pH
__ Gross Alpha __ Conductivity
11-_ Gross Beta TDS --TOC --,c --Microbiology --
--Parameter Results (Col/lOOml) --
----
----
I Date Received AUG 2 8 1997 e,). Reported by
Dcitc Extractc<l Dale Reported
I Date Analy,cd C/-i1-9..7 n,;J Lah Number 973440
1)1 IS 11 1)1 (lfrvi~cd ?/1.Jl\
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium
Chromium
Lead
__ Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachbride
chlordane
chlorobenzene
chloroform
o-crcsol
m-crcsol
__ p-cresol
cresol
1,4-dichlorobenzcno
1,2-dichloroethane
Results(mg/1)
Resu!ts(mg/i;
------
------
__ 1,1-dichloroethylene _____ _
2,4-dinitrotoluene
heptachlor
hexachlorobenzcne
hcxach lorobutadier.e
hexachloroet!ianc
__ methyl ethyl ketone
nitrobenzene
__ pentachlorophenol
pyridine
__ tctrachloroethylene
__ trichloroethylene
__ 2,4,5-trichlorophenol
_-_2,4,6-trichlorophcno!
--vinyl chloride
--cndrin
lindane
mcthoxychlor
toxaphcne
2,4-D
_ 2,4,5-TP (Silvcx)
------
------
------
I N.c: Department of Er:-..,jronmcnt,
1 lea 1th, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Field Sample Number ___ b_L-C> __ ~_~.:....:tgc._ _____ _ .~ilc Numbcr--'-Af_:_[_""-'Q--'~=..::::2-:__:S:::__S.=5:__7:_1.!.....:Cz_=----
. . Name of Site-'-(:_,_-1Jj"L-1?1-"0"'/l--=.S'--=5t'f=c..-/i_·,-=c_'---'7a,--"-'"-/1-'-'/<-c. __ Site Location SfcJesv1 //e.... U Collected By J.) W ID# ___ Date Collected CC,/2tp{ "17 Time { 7-ZS.
u Agency: Hazardous Waste. --Solid Waste --Vs u per fund TCLP Compounds
Sample Type Inorganic Compounds Results(mg/1)
D Environmental Concentrate Comments Arsenic --
13fa/ll
Barium
_· _ Ground water (1) 7r"v --Solid (5) Cadmium --. I --Chromium I --__ Surface water (2) _Liquid (6) ss-, oo / ·,e Lead --
_Soil (3) --Mercury
_ Sludge (7) Selenium I --Silver
V Othc~ (4) --_ Other (8) --
. ----f O,g,oi< Ch'"dstry Inorganic Chemistry --
I . Pnramf!(er Results(mgi!) Parameter Results (mg/l)(mg/kg) Organic Compounds Results(,,1g/l)
YP&T:GC/MS Arsenic be:uene ----1-· _ Acici:B/N Ext. Ba:-ium . carbo1: le~rachioridc ----· M':'BE· Cadmium chlordane ' ------Chloride chlorobenzene ----Chromium chloroform ------
I --__ Copper o-c,esol --
--Fluoride m•cresol --.,. Iron __ p-cresol ----.,, Lead crcso. I --------'4,~i': . __ Manganese 1,4-dichlorobenzene --,•, __ Mercury 1,2-dichloroethane .I ----Nitrate __ 1,1-dichloroethylene ----I Selenium 2,4-dinitrotoluene ----Silver heplachlor ----Radiochemistry Sulfates hexachlorobenzene ----I ······-Zinc hexachlorobutadiene
Parameter ----Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity metnyl ethyl ketone --
I --Gross Beta TOS nitrobenz.ene ----TOC penlachlorophenol ----
--__ pyridine
I Microbiology --__ tetraehloroethylene
--__ trichloroethylene
Parameter Results (Col/!OOml) __ 2,4,5-trichlorophenol ------__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrir. · --
1197 B~ lindane I Date Received --AUG 2 8 Reported by --melhoxychlor
loxaphcnc --D:ilc ExtractcJ Date Reported 2,4-0
973441: --I 2,4,S·TP (Silvcx)
Dale Analy1.cd 1~18.,qJ tJC Lab Nllmber
l)f!<.; ,1111 /llr,,,.,.,11/01\ -
N.C. Dcpartm::.nt of E,wironmcnt,
I lcalth, & Natural· Resources
Solid ·waste Management Division
SAMPLE ANALYSIS REQUEST State I...11boratory of Public Health
P.O. Oox 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
.. Site Number_M~t::,~i)~~~-Z-__ s;_S_5_7~1~Z... ___ Field Sample Number b'c"->--Z.C,'7
. . . Name of Site_S;~Jj=,' _m~o=/~IS_~X(=,c'-n_'...cc..-~~74~~/t~/c'-c. __ Site. Location Sft:i.fey 1r1 '( le...
.1 Collected By _j S ID#_-'-_Date Collected 9,/-z1s>/ q7 Time_._/c=S'-/_D __ _
0
E
I
I
I
I
I
I
.
Agency: Hazardous Waste Solid Waste v-Superfund -- --
Sample Type
Environmental Concentrate Comments
VGround water (1) Solid (5) I-a ff! bert-A (}.le ((
__ Surface water (2) _ Liquid (6) ~[)1(./ N f::.-)/yft
Soil (3) --,. _ Sludge (7) WA-Te-fc... 1,;JGU,*
_ Other (4) _ Other (8) 'S~ -d)YPW
Organic Chemistry Inorganic Chemistry
Pnrumete~ Results(mg/1) Parameter R•sults(mg/1) (mg/kg)
VP&T:GC/MS A:senic --_ Acid:B/N Ext. Barium --MTBE Cadmium ----Chloride ----Chromium . --------Copper
Fluoride ----.·. Iron· ----. Lead a ------:r __ Manganese . .. __ Mercury --
Nitrate ----Selenium --Silvec --Radiochemistry Sulfates --······~·· Zinc --Parameter Results (PCi/1) --pH
__ Gross Alpha __ Conductivity
Gross Beta TDS ----TOC --
--Microbiology --
--Parameter Results (Col/lOOml) --
--------·
Date Received AUG 2 8 1197 efJ_ Reported by
l):,tc Extracted Date Reported
Oatc Analyzed c,-1a..q, /\fJ Lab Number 973442
])I 1, '\I'll (llr~-;~,-.,t //01\
TCLP Compounds
Inorgan;c Compounds Results(mg/1)
Arsenic --Barium --Cadmium --Chromium --Lead ----Mercury
Selenium --Silver ----
--
--
--
Ori;anlc Compounds Results(mg/1)
be~zene ---carbor tetrachloride --chlordane --chlorobenzenc --chloroforw --
I o-cresol --m-cresol
I --__ p-cresol
creso: --1,4-dichiorobenzene --
--1,2-dichlorocthane
__ 1,1-dichloroethylene
__ ·2,4-dinitrotoluene
__ heptachlor
hcxachlorobenzene --hexachlorobutadiene --hexachlorocthanc --__ methyl ethyl ketone
nitrobcnzcne
__ pentachlorophenol
--pyridine
__ tetrachloroethylene
--trichloroethylene
__ 2,4,5-triclilorophenol
__ 2,4,6-trichlorophenol
--vinyl chloride
endrin · --lindane --
--mcthoxychlor
--toxaphene
2,4-D --_ 2,4,5-TP (Silvcx)
--
N.C Dcp:irtm.mt of Er:vironment,
I lc:ilth, & Natural Resources
Solid 'waste Management Divi.5ion
SAMPLE ANALYSIS REQUEST State l...aboro.tory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
.. Site Number NC.Q c:t;; Z.. SS.5 712-Field Sample Number O :Z-0,:3QC)
·. .. Name of Site S13rno/lS Stpn'c 7?.;1,/c. Site Location Sfde,sVr 'lie.. I Collected By jS ID# ___ Date Collected ca{?.to/11 T!me __ (_S_4,o~--
Agency: Hazardous Waste Solid Waste v-Superfund TCLP Compounds
Sample Type
0 Environmental Concentrate
~ Ground waler (1) -Solid (5) Tea/)e.1 ux//
m _ Surfa~e water (2) _ Liquid (6) _"1-_~D~flt~['J~{C.~f-,_c_N~fr: ___ _
_ Sludge (T) --'-[.µ--'-IJ,r.,_· =e,l_· ·_W----'-6_LL_# __
-Other (8) ___ <:::S,_-_34 __ -~R_w~_ I _ Soil{)) ... _ Othe.r.:(4)
Comments
I Organic Chemistry Inorganic Chem:stry
Juorgan;c Compounds
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
Pura meter
VP&T:GC/MS
__ Acid:B/N Ext.
Results(mg/1) Parameter
A.rse!!ic
Barium
Cadmicm·
Rtsulls(rng/l)(mg/kg) I Organic Compounds
benzene
MTBE
i I: =-----------
1 -...,•f,...1~, ----------
lr--------_.j
Radiochemistry
I J•ararnckr Results (PCi/1)
__ Gross Alpha I Gross Beta -------
, r--------_.j
11 ____ M_ic_r_o_b_io_I_ogy ____ --l
Parameter Results (Col/lOOml)
--Cbkr;cie: .
Chromiun-. ·
__ Copper
Fluoride·
Iron
Lead
__ Manganese
__ Mercury
Nitrate
Selenium
Silver
Sulfates
Zinc
pH
__ Conductivity
TDS
TOC
-------
I
I
Dale Received AUG 2 8 1197 ef:J Reported by ----------
Delle Exlraclcu Date Reported ----------------
Dale Analyzed '7 -JFJ-91 /Jr Lab Number 973443
I): 1"-: 1.11)1 (!lrvi~,·d 1/()1\ ----------
I
1
car0011 tetrachlodde
chlordane
i:hiorObenzcnc
chlorof0rm
0-Cfl'.SO!
rr..-crcsol
__ p-ciesol
crcsol
l ,4-dich!orobcn7,cne
1,2-dichlorocthane
l,l-dicl, loroethylene
2,4-dinitrotoluene
heplachlor
hexachlorobenzene
hexachlorobutadiene
hexachloroetha:ie
methyl ethyl ketone
nitroben1.cne
__ 1,enlachlorophenol
pyridine
tetrachlorocthylene
__ trichloroethylenc
__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol
vinyl chloride
endrin ·
lindanc
mcthoxychlor
loxaphcne
2)4-0
2,4,5-TP (Silvcx)
Resalts(mg/1)
Results(mg/1)
-------
-------
-------
------
------
------
,N.c: Ocputmcnt of En·,ironment,
l lcallh, & Natural Resources
Solid Waste: Management Division
SAMPLE ANALYSIS REQUEST State L..11.borato1y of Public Heal1h
l'.O. Box 2S047, 306 N. Wilmington Street
Ralc:ig.h, North Carolina 27611
wile Number NCO ~ z_ s-SS 71 z... Field Sample Number 0---z-0?:,o(
. Name of Site ':Jjl11.0/I S $q?kc.-7?!,/l/c_ Site.Location Sfq.}ey /// / /e__
. E Collected By J.S JD# ___ Date Collected e(vs(i:11 Time I "i??o
I Agency: Hazardous Waste Solid Waste --Vsuperfund TCLP Compounds
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
(?e(ow Ldi¥1 /:R.rt:A Barium --Cadmium __ Ground water (1) _ Solid (5) --
I ps0-cl Chromium
VSurface water (2) --_Liquid (6) Lead --ss-( (0-S,l)J
__ Mercury
_Soil (3) _ Sludge (7) Selenium I --Silve1
_ Other°(4) --_ Other (8) --
I --
--Organic Chcm:stry Inorganic Chemistry --
11 Pathmeter Rcsults(mg/1) Parameter Results(mg/1) (mg/kg) I Crganlc Compounds Resulls(mg/i)
VP&T:GC/MS Arsenic benzene . I _ Acid:B/N Ext. --I -· Barium ca~:::>or, tctrachlorij:; ----MTBE --Cadmium chlor~ane ---·-Chloride chlorobcnzene --------Chromium chloroform ---·
I --__ Copper a-err.so: ----Fluoride rr.-crcsol ------Iron p-c,esol -· ------> Lead c:eso1 I --
--· __ Manganese 1,4-did:lorobcnzenc
I --., __ Mercury 1,2-dichloroethane ------Nitrate __ 1,1-dichlorocthylenc
I --Selenium 2,4-dinit rotolucne ----Silver _. _ heptachlor --Radiochemistry Sulfates hexachlorobenzene
I ----...... -,. Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachlorocthane ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Beta TDS nitrobenzenc ----TOC __ pen,achlorophenol --
--__ pyridine
I Microbiology --__ tetrachloroethylene
--__ trichloroct,,ylcne
Par~1mcter Results (Col/1001111) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichloropncnol
----. --vinyl chloride
e~drin --
1997 ~eportcd by
lindanc I Date Received AUG 2 8 --methoxychlor --
--loxaphene
Delle Exlraclcu Dale Reported 2,4-0
I --
973444 2,4,5-TP (Silvcx)
Dale Analyzed C/-18-C/7 JJt Lab Number
' .. ' < --])I IS JI )I (llC\ISCd __ /)l'\
1. i\'.C: Department of En·-.'lronmcnt,
l lcalth, & Natural Resources
Solid Wa~lc Management Division
SAMPLE ANALYSIS REQUEST St11.lc Lebort.tory of Public Health
P.O. llox 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
.... ,ite Number /VC,/) Q;; 2.-s-ss 712-Field Sample Number 07-0s.oc...
Sf des VI lie.. Name of Site ~t . I ~·kc 7a.Alc.. Site Location -13rno/lS
I Collected By JS ID# D_ate Collected 0(-zotq, Time (3,{o
I Agency: Hazardous Waste Solid Waste VSuperfund TCLP Compounds -------,-··--. --..
' Sample Type Inorganic Compounds Resuits(mg/1)
I Environmental Concentrate Comments Arsenic --Barium Ett u i r {))ef\} ---.-Ground water (1) _ Solid (5) Cadmium --
I Chromium ~(\..')~ 13/o.f\ I::-----__ Surface water (2) _ Liquid (6) Lead --
s.s---'?,;co-RE,
__ Mercury
I _ Soil (3) _ Sludge (7) Seienium --.. Silver '·' --__k::_ Other,(4) _ Other (8) --
I --
--Organic Chemistry Inorganic Chemistry I-.
I Parumctcr Results(mg/1) Parameter Results(mg/l)(mg/kg) i Organic Compounds Resulls(mg/1)
VP&T:GC/MS Arsenic · benzene --t-Acid:B/N Ext. Barium carbo.~ ~ctr:.i-:hioride --I --· MTBE . Cadmium . cnlordane ---------. , Chloride· chlcirobenzenc ----I --Chromium ci1;0;oforrr. ----
E --Copper o-cresol. --I --Fluoride m•cre1'o: ----' --
--Iron I -· p-cresol --' Lead creso! E --·""· ----l{'f '. __ Manganese I l ,4-didiiorobenzer e ----{.\ __ Mercury . 1,2-dichloroethane --
--Nitrate __ 1,1-dichloro<;thylene
E --Selenium 2,4-dinitrotolucne ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene
E ----······-·· Zinc hexachlorobul ad iene
Parameter Results (PCi/1) ----pH hexachlorocthane ----__ Gross Alpha __ Conductivity . __ methyl ethyl ketone
0 --Gross Beta TDS nitroben1..cne ----TOC __ pentachlorophenol --
--__ pyridine
0 Microbiology ----tetrachlorocthylene
--__ trichlornethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol · --
~ ----__ 2,4,6-trichlorophenol
--__ vinyl chloride --endrin ·
. J) --lindane
D AUG 2 8 1997 8 Reported by --Date Received methoxychlor --
--loxaphcric
D:llc Extracted Dale Reported 2,4-0
0 -----------1: __ 2,4,5-TP (Silvcx)
Date Analy-1.cd 1'-1P,-q1 NT Lab Number 91J4'1'4,'
1)11'-: 1\l/1 (H,-v;(,•d ?/•Jl\ --
.. ,.p,,·
STATE IABORATORY OJ.I' PUBLIC HEALTH
PO BOX 28047 -306 N. WILMINGTON ST .• RAIEIGH. NC 27611 .. ORGANIC CHEMICAL ANALYSIS
' q13'-/Jr q,3'-12.B crr3'-!2q q73430 973431 Q7.3':-/2bl.. I PURGEABlE COMPOI/NDS LAB NO
FIELD NO 2026'{ o20.2es . 202B& ;lOdJ8 7 ;zo;;i_,gg-ol-0'2~/
I COMPOUND TYPE C I ) C I ) C I ) ( I ) C I ) C I )
~g/;)~ 'PP b) ppm 'rl'b ppm; / ' (opb l?pm "ppb' ppm. ",;pJ,)r:prr, C . fY'b ppm
I CHLOROMETBA1'11! JO (.,L. II , , LL LL I I I
VIN'TL C;HLQRIDE 10
BROMOIIIETHAMJt ;i.o I CHLOROETIL\N'B 10
TRICHLOROFLUOROll&THAJ'IE ,o . / I // ," ,[/ ,I/
I ACETO IOI: . .;J.0 (o 4::; 99 5 106 -:r J93 j '70 :r 31 J
1.l•DlCBLOROETHEN"E 5 u.... I I LL /J u_ LL,
i
'
I tOOOIIETHA.llE ~ +rti C, Jim'I'IITLEl'm CHLO RIDE rP_
I CARBOPI DJSUI.l'IDE LL
TRAlffl-1,2-DICHLOROETHEI'm ' ,
~~== ;lD ' I
' ' / ,,,..
5 0,5':r 0-4 ::r s
1-DICBLOROETBANE I
3-BtrrANO?m ;10 I ' / j LL
I CIS-1,2-DICHLOROETHEIB 5 ~ s 0 . :r ' / ,;i_':1' • lo
CBLOROJ"OR.11 I I 0, lD ':1' +ro.Le__ u__
I 1,1,1-TRICBLOROETHARE u..... I I
CARBOff TXTRACHLORIDlt ' I . / I/
I 1Ya.ce,_ '+ s 3 :r BEJm:IOI: 0,
1,2-DICHLORO~ I I I ' Le
I TRICBLORO~
1,2,DICHLOROPROPAKE
BROMODJCHLOROMETHAlfE ' , \ I '• , \ / ,/ ' ',
\ I
I
I
C • ,p.,:,,s, 6~ I.II & <:o..rt"ll~1II ATION oR 8Ac.l..6R.ou.i-A D.
J -ll:■timat■4 TalU■ /
K -Actual value i• known to be l••• than value given.
L -Actual value ia known to be greater than value given.
U -Mat•rial was analys•d for but not detected. Th• number ia th• Miniau:m Deit•ction Limit.
ID. -l!ilOt analys•d. .
1/ -T•ntetiv• identification.
I a:, -CD' ~!'011.l'lD RB.I l'leL"f•D~R8Lf.. oHU( '"' /116H CCINC£Nmtm~. ✓-S~PLli. Hl~L'j OILkTliO, ~OL.'~ 0o tlo'r' ftf'f>Lf. ·. ·
DEHNR 30815-0 (10/93) l'URGCOM.ORG 1· .~·<(\: .. :..,,•-;,,_,.. ·._,. ,:;
~·:;.;:1:~-~; . ,:;, •,. :,·; i .:.J 1.?_;:,•,;'· ·,· ·1 fJ.,':,' I
. ' . . . . . . . . . . ~ -'ii~, ,I.~.,;,~ 1.i·~,;5~'.C·~-~};J~r.:i:b~ . : _; ~ff~ff~€,;/)~; .. fif {t0! "'.'. ''
I
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STATE LABORATORY OF PUBLIC HEALTH
PO BOX 28047. 306 N. WILMINGTON ST •• RALEIGH. NC 27611
ORGANIC CHEMICAL ANALYSIS
P!JRGEABU: COMPOIINDS LAB NO q134-2'1 973428
FIELD NO
COMPOVND TYPE ( I ) I I ) n~~:, 'ppb· 'f't)ffl MbJ,f'P/1'.l
DlBROMOMETHANE 5 {,L...-I
4-METJITL.2"'PENTAI'l'O?m ,o
CIS-1,3-DICHLOROPROPEKE 5
TOLUEn
TRAl'fS-1,.S-.DICHLOROPROPEn
1.1.2.2-TETRACHLOROETBAlfE
l,1,2-TRICBLOR0ST11Al'(g ' /
2"'HE.L\J'l'OKE /0
TETRACHLOROETIIEl'llt 5
DIBROIIOCHLOROMETHANE
ETHTIZI'fE DrBROII.JDI!: ,/
CHLOROBENZE?m f,,-ace_.
1, 1,1,2-TETRACHLOROE;TJL\ffE LL
l:TH1'L BEl'l'ZEKE J,,
rru:ns +-raa:~
9TTRUE ' I I '
BROIIOFORll iO
TRAlfS-1,4-DICHLOR0-2-BUTEl'f!: 550
1,2,3-TIUCHLOROPROPANE 5 '/
1,,&.DICBLOROBE?raE1'(J; I o.+ :r
1,2,DICBLOROBENZElfl!: ,Lt +V""o.c_e.,
1,2•DlBROM0·3-CHLOROPROPANE ,;i. t) I •
VINYL ACETATE ;i..cio ' I J,
:r so Pr<>Du I ale.oho\ y ®tr-"J E) E)
c-l"0,;5\8'-'!. 1..1'\I!> O>J'TRt,l.i~flilON oA 5ACl;~O\UIIO,
J -Batimat•d value
K -Actual value i• known to be l••• than value given.
L -Actual value i• known to be greater than value given.
cn:Y+zq
( I )
ppb')pp,r
. I •
' '
+rrlce-
LL
.J,r
,,;;i_:r
I •
,1
o, B ::r
J--,rv'°
l,L.., w
8
Q73'+3o C/73'+31
( I ) ( r i
/'ppb).ppm /~t,,.ppm;
11 I l
,:i-
LL-
+ra.ce....
; I
' /
31
L-L
O•d. .r
4s
(.,L
\ v
q
13
(.,L
' I ,\,
g E)
0 -llatarial wa• analy.a:ad tor but not detected. Th• number 1• th• Minimum Detection Limit.
lD. -Rot analysed.
1/ -Tentative idantitication. :a:, · c:oMPoLl,.SD, Rei;1Aei..y P6fcer-Ael.E. :ClllL'( 1/J · t-116-H co1,l((NTRAT!otJ5,
,/-SA/14PLI; H16·Ht.Y l)ILLlTED. MDL~ DO~ APPLY,
DEHNR 3068-0 (10/93) , ':,"' ....... _ ... . ::i!;~,.
q13'f:P-
(_\ )
,, ppb Jpp,rJ
LL-
\/
(8
l"URGcOM.ORG /
STATE IABORATORY OF PUBLIC HEALTH
PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH, NC 27611 .. ORGANIC CHEMICAL ANALYSIS
PVRGEAIILE COJIIPOVNDS LAB NO q13433 q734-34 q7_3Lf35 97343(.;i G/73L/37 . . ..
FIELD NO ;;20.)40 olD.19 I ,,20;;29~ .,2a;:i_q3 :1f);).9 '+
COJIIPOIIND TYPE ( .2 ) ( .2 ) ( ,;,_ ) ca l ( .;z )
m ':1,,~t;;" C . -pp&)pp,n ~b~Jp11m tppb}pprn ~pm (P(Jb ppm
0 CHLOROMETHANE JO J A I I I I I I l
VINTI. c_HLORIDE 10
BROIIOIIETHANE ;io E CHLO RO ETHANE 10
TRICHLOROFLUOROIIETBAl'l'E ,o :../ ' I \ I ' I ,I
I ACETO in: .. .;;2.0 3.;;). :::r ,,J..'1 j IJ. -r J4.:r 9i:r
1, l-DICHLOROETiml'fE 5 I I Ll---I l I
I IODOIO:THAffll;
, I MZTBTIZN'lt CHLOIUDE
I CARBO!I D1SUL7IDE +r/\re,,
TRANS-1.2-DICHLORO~ ' I / J
ACRTI.Olffl'RllZ ;;lD
1.1-DICHLOROSTBANE 5
3-BUTAR'OR ;;l.O
I CIS-1,2-DlCHLOROETHENE 5
CHLOROFORM
I l, l, l •TRlCHLOROE'l'llANE
CARBON' TETRACHLORIDE
I ,mm;,n:
1,2-DICHLOROETHA!'fE
I TRICHLOROETH.cl'(E
1,2-DICHLOROPROPA!'IE
' I
,,
I
I
BROIIODIClll.OROIIETHANE ' I ', 21 '
" ,£1,
I '1J -c
C-.Po"'5164' l.#l&CO.rffl~IIIRT"ION oR 8Ac.l;.6~o u» o.
J -&atimated value
L -Actual value i■ known to be greater than Talue given;.
'
K -Actual value ie ltnown to b• l••• than Talue given.
a -Material waa analysed tor but not detected. 'l'h• number i• th• Minimum Detection Lilllit.
ID. -Hot analped..
1/ -Tentative identification.
I !I -CDl'\l'OIAl'\D. RB.1AeL'f·OloTl:CiR8LE-oMU( '"' fll6H_~H~cNS.
✓-SAl'IPL& Hl~L.'( DILllTI.O, ~OIJ,o Do ~ AfPL.f,· . .
I
DEHNR 3066-0 (10/93)
.
I 1 -
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.· .. l ·0•· .. ·.···.?
C/7 3L}-"3fj
<i2U;295
I ..:2.l
l/ppt,}a,rr,
I
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I"· . :(.:-. ; ::fli~:;iiii·R:~\~;:~~}~~~1At-;F: ... . .
-.t:· fP\?f1' \ --~~t{.::•·'.:-. · :. ,.:.,,,_~·~·:•.-· . .-· ·
STATE LABORATORY OF PUBLIC HEALTH .. PO BOX 28047 -306 N. WILMINGTON ST •• RALEIGH. NC 27611 .
ORGANIC CHEMICAL ANALl'SIS
I
I
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D
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I ,,
I
I
PIIRGEABLE COMPOUNDS IABNO q,3't33 9 73 '-131-\-
FIELD NO
COMPODND TYPE ( .,2 ) ( ;z_ )
no6)5 ~Pb lppb ppm (pp~)f'p/f'.l
DIBROMOMETHAl'IE 5 I l I I
4-METHYL-2-Pf:NTAKON1t ,o
CIS-1,3-DICHLOROPROnNE 5
TOLUEl'IE
•• ' > ~ •• . .. " TKAl'fS-1,3-DICHLOROPROPENE
1.l,2.2·TETRACRLOROE'I'B.AlfE
1,1,2-TRICBLOROIC'tllAffE / '
2--H!tLVl'OKE /0
TnRACBLOROETBlt!m 5
DlBROIIOCHLOROlm'THANE
ETHYLE?O: DIBROIIIDE
CHLOROBENZEI'fE
1.1,l,l-TETRACHLORO~E
ETHYL Bm'l'ZEJ'fE
JCTLEIIES
STTIW<!: 'I
BROIIOFORM ;o
TRAffS-1, 4-DICBLORQ-.2--Btn'El'CE io
1.2,3-TRIClll.OROPROPANE ..5
1,4-Dicm.oROBEffZEIB I
1,2-Dtcm.oROBEN'ZENE -Lt
1,2,0IBROM0-3-CHLOROPROPAR ,J.E>
:x>O ' J '\ I
V1N'TL ACETATE
I'..:x,oro{)t/ I a. koh.cJI J/ cD1c1 CB (-)
c-,~el.I;. I.FIB 0>14TFl1'.1Nfli10t,I OR 13Ae1;~oui.10
J -l11timated value · '
X -Actual value 1• known to be l••• than value given.
L -Actual value 1■ known to be greater than value giv.n.
"
q73'--135 q 73431.o q73J.f31
( c2 ) ( ,;z ) ( o:z )
lpb}ppni /4b') P , ppm mv'Jppm:
I 1 1 I
'
/ . ' I
O,lD ::r 0' &, ::r
"·*··•.' •' ·-, .... ~-, • . e,c;· I l
' I \ I
(-) (-') (-
O -Material wa■ analyzed tor but not detected. Th• number i• the Hinimma Detection Limit ..
ID. -Hot analysed. ·
1/ -Tentative identification. It -C:OM~Ut,10. ft1:1;1ABL'f P6TECff\SLE. t~LV IN H16-H ccr,ICCNlRAT10N.:;,
/-SA/I-IPL!:'. l-116-HLY l)ILUTED. MDL~ l)O JsloT" APf'1..:y.
DEBNR 3088-0 (10/93) . -ttYi~It;~~fti~•~.:-.:r"'~,:-,.(:_~fr;_.;it,t"-Jr;~ .~;'_~_;",:; .'• .. _.,.,:iJ\~~~~ :···:.,.
'l'f3"!38
( .2 l
ftJe!VPPlll
I I
··•,•· . ·· .
¥
( _;))
----,-.-:,~~·-----··.
STATE I.ABORATORY OF PUBLIC HEALTH
PO BOX 28047 -306 N. WILMINGTON'ST., RALEIGH. NC 27611 .. ORGANIC CHEMICAL ANALYSIS
I PVRGEABLE COMPOUNDS tABNO <n3'f3C, q,3'-Ho C/73'-t-4-1 q--, 31-/-Lf;l_ q73'-f'f3
FIELD NO .;J.OJ_q(p ol.0;297 .2QA'ir ,;,__O;AC, ol.0300
I COMPOUND TYPE ( ,;i.. ) ( I ) ( '-1-) ( I ) ( / )
':\,~!;)" tPf>l:>)ppm_ 'rPb)ppm. / ppb ppm / :--/J. (ppb')ppm_ C . ppb pm
m
CHLOROMET'HAl'B J.O ,L I L,L L..L LL
VINYL C:lfl.ORIDE 10
BROMOIIETHAl'fE ;20
0 cm.oROETHANE JO
TRICHLOROFLUOROK&'T11Al'f!; 10 ' / ' I ' I ,/ / .
~ ACETOrn: . .;i.o 10 ':5 II 3 8 -:s 84.J ~ I :r
1.1-DICHLOROETHEl'fE 5 {}..... LL. 11 L,L.... J
I IODOKETHAl'l'E t-
{}_ ::T,C--
JBTBTl.ZffE; CHLORIDE
I CARBO?f DISULFIDJt (A_.-
TRAl'IS-1.l•DICHLOROETHEI'fE ' /
~RTLO-=
;;2D
1-DICHLOROICTHAl'fl!: 5
:J.-BOTAKO?fE ;to
I CIS-1,3-DICHLOROnHENE 5 \ /
CHLOROFORM +r"' cP
I 1,1,l·TlUCHLOROETHANE / l -
CARBON TETRACHLORIDE
I IWIZErn:
1,2-DICBLOROETB.Al'l'E
I TRICHLOROn11..ilfE
1,2-DICKLOROPROPAJU
BROMODICHLOROIR:'l'llA.NE ' I ,/ ·, I ' / ' I ,/
I
I
C-.f'o:>S•S~ I.I'& <:oNTfl1'11IIRT"lO!II oR 8AC.!;.6~ui-AC.
J -Kati.mated value
K -Actual value i• known to be le■■ than value given.
L -Actual value ia known to be greater than value given.
O -Material wa■ analysed for but not detected. Th• number i• th■ Kinimum Detection Limit.
111A -Hot analysed.
I
1/ -Tentative identification.
°II -COl'\Po1o1J!lo. REUf\£1L'f'•0£ftCJ"l'l5LE. O,.Cf '" 111611 ca«£NrR,il"loN5,
✓-SAAPL& Hl~Ly QILll-rao, ,401.!~ Do~ f'lfPL'(,
ilEHNR 3065-0 (10/93)
. i
q73'7 '-f 4
;lo.301
( .;2 )
V pp/J' ,:Pl") I
!
I , i
I
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ll.o.J"
IL-
' (
PURGCOM.ORG
STATE IABORATORY OF POBUC HEALTH .. PO BOX 28047 -306 N. WILMINGTON ST •• RALEIGH. NC 27611
ORGANIC CHEMICAL ANALYSIS
I
I
I
R
E
I
I
I
I
1. i'
I
I
I
I
PVRGEABLE COJIIPOUNDS LAB NO Cfl 3'--f 3Cf q73'-f 40
FIELD NO
COJIIPOVND TYPE C.2) ( fl )
t 0f{' ,pt, vppbJppm lppli}_f-Plt'.ll
DIBROMOMETHANE s ti I l _
4-METHTI.-:J..PENTANOlfE ,o
CIS-l,3-D1CHLOROPROPENE 5
TOLUEl'R:
TRANS-1,.S-DICHLOROPROPENE
l,l,2,2·TETRACHLOROE1'HAllE
1.l,:J..TRicm.0ROETHAl'O!: ' /
2--HE%Aft'ONE /0
TETRACBLOROETBE1'E 5
DIBROMOCHLOROlmTHANE
R DIBRQMIJ>g
CHLOROBEN'ZEffl:
l,l,l,2•TETRACHLOROETHA!'l'E
l:THTL BEft'ZElfE
XTLEl<ES
STTRE!fE ' I
BROIIOFORII iO
TRAlffl-1,4-DICHLORO-:J..BOTENB <to
1,2,S-TRICHLOROPROPAl'IE .5
l,,&..DICBLOROBENZEN& I
1,2,Dtcm.oROBEN'ZltNlt -v
l,2-DIBROM0-3-CHLOROPROPANE ,;I. E)
vnrn. ACETATE ;;)..C)Q ,/ ' I
:X.:;oprop~ / a.I coho ( .!/ {BJ?) ~) (--
C-1"0"5!8~ I..JqB O>~tl.l~flj\ON OR i3A0.8ROUN0, J -Estimated value
g -Actual value ia 1tno,m to b• l••• than value given.
L -Actual value i ■ known to be greater than value giv.n.
qi 34:'-/:( 973'-14~ q734'-f3
( Lj ) ( I ) ( I l
,/ b) PP Pptfl /p,,li);p.pm ,Pb}pm
/ I I' I -
I
' (
-+('QQ....,
U-
' / \ I . I
~) (-') (~
U -Material waa analysed tor but not detected. The number i• the Minimum Datection Limit.
ID. .. 5ot ana.lys•d.
1/ .. T•ntativ• id•ntification. It -cOMPol.ltJO, lttLIAeLY P6TEGT-A0l.E. tl.JW IN t-lili-t-1 cc1,1CCNlRAT10N:.;,
✓-SA/1-lPLlo 1-116-HLY [)ILLlTED. MDL~ DO>JoT" Af'f'I..'/,
1 .. DEHNR 3068-0 (10/93)
· .. 4-·~:;¢,~ii:~J;~~•·: \ • .. '. ,, ; .. , ..... ' . :, •\ ·, .~.
q73L/4'-f
( ,;2 )
/ ' ,} ppb ppm
I I
-';'"<•' ~: ·, c,; •!fc J
', r-
•' . ,).,.'"J::~· ;-i• ,.
I srATE LABORATORY OF PUBLIC HEALTH
PO BOX 28047-' 306 N. WILMINGTON sr .. RALEIGH., NC 27611 .. ORGANIC CHEMICAL ANALYSIS
11 PVRGEABLE COJIPOUNDS
I
LAB NO 1::3;:~ I I I FIELD NO
COJIPOUND TYPE . ( )..j ) ( ) ( ) ( ) ( J I ~~Ii·? C . (,,pl, pprn. fl>b.ppm: ff>b ppm ppb pprn ppbpprrt
I CHI.ORO~ JO J
VlNTL C_HLORID!; 1n
BROIIOIIETHANE ;io·
ClD.OROETHANE 10 .
TRICBLOROFLUOROKP:T'HAl'fE ,o \ I
ACE'tOl<I: . .;;io ,--,s
1,l•DIClD.OROETBEB 5 I I
I IOOOlmTHAKE
IBT!l!'IZNE CJD.ORIDE
I CARBON DISULPtDlt
TJlAl'l'S.-1,2-DICHLOROtrHENE ' ' t,:;== ;;2D .
·DICHLOROln'HANE 5 ' I
2-BtrrAft'Ol'B ;>.O 3::r
I CIS-1,2-DlCHLORO~ 5 l,L
CHLOROFORM -/-r,,rP
I 1.1,l•TRICHLOROrrHAlfE I •
CARBOl'I' TETRACHLORID!:
I BENZ!:IB
l,2-DICBLORO!:TBA1'fl!:
I TRICHLORO!:TH.Ji]U
1,2-DICHLOROPROPANE
' /
BROMODICfll.OROIIETHANJ!: \ I I
I
c -.Po:os, e~ '-II e co.rr11~1i,1 RnotJ oR 8Ac.l;.6~utJ o.
J -Betf.mat•d value ,,
Jt -Ac:tual value is known to be l••• than value given.
L -Actual value ia known to be greater than T&lue givan.
O -Material waa analyzed for but not detected. 'l'he number 1■ the Minimma Detection Limit.
ID. -Sot analyzed. .
1/ -Tentative identification. ·
I It -CD~1'01.ullD RELIAl\L'f0ETf.Cr1'15LE.: Orf~ IN 1116H C&lNC.£N~oNS. ✓-SNIPLt. Hi"iiL'f DILL,:T~o. ~OL'~ Do~ PtfPLy.
DEHNR 3085-0 (10/93)
I · . ··.ai·"''ii[ih•, : · .. ~~,:~h,;.f~;fjtr ... ,
.. --,.--,'.-1~<'.·'. ~ ;t.fbr{J.,~; '\(~t',/:f't~·"
I I
( )
ppt, :all".)
Pl!RGCOM.ORG
srATE IABORATORY' OF PUBLIC HEALTH
le PO BOX 28047 -306 N. WJLMINGTON sr., RAIEIGH, NC 27611
ORGANIC CHEMJr'AL ANALYSIS
m1 PURGEABU: COJIPOVNDS
I
lAII NO I q1344SI I I I FIELD NO
D COMPOUND TYPE ( 4 ) ( ) ( ) ( ) ( )
(J~f{' ~Pb 'ppb')ppm ppb ,f-PIO ppb Pf3t(! ppbµpp,ri ~Pppm;
~ DIBROMOMETHANE 5 u.....-
4-METHl'L-2-PENTAl'ION'E ,o \
I CIS-1,:l-DICHLOROPROPENE 5
TOLU!:l<E
I TRAl'fS-1,:S-DICHLOROPROPKNE
l, l,l,2-TETRACHLOROETIL\lfE
I 1.1.2-TRJcm.oROETHAl'flC /
'
2-BEL'l.ffOlfE JO
TETRACHLOROETIRR 5 I DIBROMOCHLOROMltTBANE
ETHTLEl'IE DIBROIIIDI!
Clll.OROBENZEl'flC
l,1,1,2-TETRA.CID.OROETHAffE
I rnrn. BE?fZENE
rru:im,
I !ITTlW<l: ' I
BROIIOFORM iO
f TRAl'fS-l,4-DICHLOR0-2-BO'TEIU <to
1,2,S-TRICHLOROPROPAl'fE !5 '/
1,4-Dlcm.oROBENZBHB +.,.-alP _ I 1,2-Dtcm.oROBEN'ZENE ,1 1.)..-,
1,2-DIBROM0-3-CHLOROPROPANE ,;it)
t VIl'fTL ACETATE ;;)..CJO , /
:C.sof>ropy I oJ tohol _i,, ffi/E) R--)
I·
K -Actual value i■ known to be l••• than value given.
L -Actual value i• known to lM; greater than value givan,
·a. C-1"~8'-1!. I.FIB O,l{TI'lt,11 ... piloN OR 5'\Cl.~OU!IIO, J -latima.t•d value
O' -llaterial wa■ analya:ed for but not detected. 'l'he number i■ the Minim.um Datectioii Lia.it.
I
I
D -Not analyzed.
1/ -Tentative identification. a1 -COMPou.t,10,.Re1:1ABL-Y 06ice.rAeU:: a,,w, JN t-11Cr-H coNCCNTR1n-10N.:;, ✓-SAl'lPLf'. H16-HLY t)ILUTED, MDL~ l>O lllOT" APPi..'/,
DEHNR 3068-0 (10/93) : ,·
I I
( )
ppb PP11J
l'URGCOM.ORG _;
,, •
1Nco'il1•iNR
I Division of Waste Management
cgr · Superfu'nd Section
Organics Lab: L-
Inorganics Lab: __
D Hazardous Waste Section
.. D Solid Waste Section
I
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CHAIN OF CUSTODY RECORD
Project Name: ":::i~fY!u/75 ?f3/1:'c 1zu1/c.-Sampled By: Col'l /V\.... ()_; r' ls.oV\
Site ID # (NCD#) N c._'f) oS Z-5~ 7q Z-· Sampler ID
Location: Smfesvi !Ir. /\JC Telephone:(q{9) 7 53-7-Rio/ qd-317 Address: /7/4'3 Ev.fut;.._ /2.4-Date Sampled: <0{z.s£r1, C3/u(11
Time Sampled:
Sample Types: Soil v Water Waste L/ Other
Remarks: ,<:,n~ es i f\ci( ecJ <-J.. w I rt\ (lS.-k ri L £'.l( ~ (,<.)G'>.i e., VJ rcvC u c._+ (i NI usir I o..l resl de~-\-\'o-.\. 1 s,~ s.lu~Q_') ('hJc)e, %-b'-ilc-' J.' qt '{ lf:f\A I ({\ · lC "~ S,b[ -
U-X). 'i,~ PID J (J,_ d---
Field Sample Cfk.3" -z,/ 0"2.D~2-Z., C>J-63>-z.,3. o·zz,~?4 o,o"s.Z::. oz.a ~?I,, crz,o?;Z..,
Numbers 0"2.a ~Vo 0'20?,;Z':f_ OZC>~'30 1-t,1,.e:, ?:.~ ( fl;L-e) ~ *0·2..o3,3,3, 1'-07-0?,o/f::
¥-{'.)'Lb s~.S ~0'20~ o?.0?>'31 02a'c,~ Cf2b~3"7 cFZ-o?f(0 0 --ic-c:4 :!
02-0'½--'2-c:R.e:,~.?. *9"2-o344
I
ft
I . Relinquished By:( ),1,ef,., T,t,t, \..pl'7a-1I 9;,' _;/ A Time: lS JO Date: r-)l'7 1
'
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I
/Sion1.;c)
Received By: C )1//f,) U, -
(Signature)
Relinquished By:
(SiE.11rnture)
Received By:
(Signature)
Relinquished By:
(Sienature)
Received By:
(Signature)
Results Reported:
(Signature)
I I " /)' e~.-Date: ft-2-f','?7 Time: L,;-:10
Date: Time:
Date: Time:
Date: Time:
Date: Time:
Date: Time:
I
,, ,.
· N.C. Uv,)artmcnt of Environment,
I lc:illh, & Natur.il Resources
' Solid \','~isle Mc\nagemenl Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
PO IR~ !JO{,ll't•Mhpi1gt~n Stccct
~(elgh·, Nlr&:Carolma 27611
Field Sample Number __ ~o~·~-z._.o_~~fil.; __ f"~f_2-"-3-'lC:C9""97,__ __ _ I .itc Number-'-M-'-"c,=o'-00=-=-z....=----"--s_s-=-5-----"-7--'--1_2... __
' Name of Site_SJ_&,_,'"l'm-'-'-"'o"-//'--'S"-
1 ___,Yf="--/ic:....:::'c..,::::___,]4'-""!_/1::.c/c.~_ Site Location Sf,:;..,,/-ey VI'( fW.PERFUND SECTION
I Collected By j 5 ID# ___ Date Collected s /2.S( q7 Time ;s--zo
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Agency: Hazardous Waste Solid Waste Vs u per fund ----
Sample Type
Environmental Concentrate Comments
Se,://mer, +-. be(ow· __ Ground water (1) _Solid (5)
/
__ Surface water (2) _ Liquid (6) ?PE
. v' Soil (3) _ Sludge (T) <;,S -D-7 -Si)
_ Other (4) Other (8)
Organic Chemistry Inorganic Chemistry
Purnmctcr Rcsul!s(mg/1) Parameter Results(mg/1) (mg/kg)
-VP&T:GC/MS Arsenic --
Ac;d:B/N Ext. --Barium
MTBE Cadmium ----Chloride --·----Chromium ----
----Copper
Fluoride ----Iron --· --Lead ----
--__ Manganese
--__ Mercury
Nitrate ----Selenium --Silver --Radiochemistry --Sulfates
I ······-·· Zinc --Parameter Results (PCi/1) --pH
__ Gross Alpha __ Conductivity
I --Gross Beta TDS --TOC --
--Microbiology
I --
--Pan.1mder Results (Col/l00ml) --
----
----
I Dale Received AUG 2 8 1197 so Reported by
D:itc Extracted Date Reported
I. 9-;;z3-q71-l:r 973446 D:itc i\naly,cd Lab Number
!)II'-: 11()1 /11,,v;,n! ?/1)1\
TCLP Compounds
Inorganic Compounds Resu:ts(mg/1)
Arsenic --Barium --Cadmium --
Chromium --Lead --Mercury --Selenium --Silver --
--
--
--
--
Organlc Compounds Results(mg/1)
ben1.enc --carbon tctra-:hioride --chlordane --chlorobenzene --chloroform --o-cresol --n:.creso: --
--p-cresol
crcsol --1,4-dichlorobcnzene --1,2-dichloroethane --__ 1,1-dichloroethylcne
2,4-dinitrotoluenc --__ heptachlor
hexachlorobenzene --hexachlorobut adicne --
hcxachloroethane --__ methyl ethyl ketone
nitrobcn1..c.nc --__ pcntachlorophcnol
--pyridine
tctrachloroethylene --
__ trichlCY.oethylenc
__ 2,4,5-trichlorophcnol
__ 2,4,6-trichlorophenol
--vinyl chloride
endrin --lindanc --methoxychlor --toxaphcnc --2,4-D --
2,4,.5-TP (Silvcx)
---
' E .', N.C. Dupartmcnt of Environment,
I lcallh, & Natural RcsoJrccs
Solid \1./astc Management Division
SAMPLE ANALYSIS REQUEST State l....aboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North CarolinJ1 27611
.. ite N umber_:._M.:::L-""""-L)---'00::.£.:::z.__:__:s;=-.c:.S:=:5:__:7:...1-'--""Z...'---__
Name of Site S,,jlmo/1.5 S:,7kc... ffi/l/c._ Site Location Sfqjey //i '//e_
CoHected By ___ ___:<...\:=:, __:s:::_ ___ ID# ___ Date Collected f3(z.S( tJ1
Field Sample Number ___ 0_·_7,_.(:)_3_z_·_z... _______ _
I Time /</-10 ------
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds ----
-Sample Type Inorganic Compounds P..esulls(mg/:)
I E1,vironmcntal Concentrate · Comments Arsenic --
,~,? Ji (Y\~/\,+' loo:dc~ r«N'-
Barium
__ Groundwater (1) _Solid (5) -Cadmium
' Chromium I __ Surface water (2) 'D0'\{.l --_Liquid (6) Lead --l __ Mercury
I JL::_ Soil (3) _ Sludge (T) S:, ', -c) 'o -St) Selenium --Silver --
_ Other (4) __ Other (8\ --
--I --Organic Chemistry Inorganic Chemistry --
I Paramc!cr Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Rrsults(mg.i:)
YP&~':GC/MS .. Arsenic benzene ----Acid:8/N Ext. Barium carbon tetrachloride ----MTEE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform -------
I --__ Copper o-crcsoi --
---Flu0ride m-crcsol ----
--Irm .. p-cresol ----
I .-,-Lead crcsol ----
--__ Manganese :,4-dichlorobcnzene --
--__ Mercury 1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylene
I --Selenium 2, 4-dinitrotoluene ----Silver __ hcptachlor --Radiochemistry Sulfates hexachlorobenzene ----I ······-····-· Zinc hex a ch I orobu t a<l iene
Parameter ----Results (PCi/1) pH hcxachloroethane ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I ·--Gross Hcta TDS nitroben1..cne ----TOC __ pentachlorop\1enoi --
----pyridine
I Microbiology ----tetrachloroethylcne
----trichloroethylene
Parameter Results (Col/JOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --
I AUG 2 8 1197 ,e,.OReported by
lin<lanc
Date Receive.cl
--__ mcthoxychlor
__ toxaphene
D:ilc Exlracted Date Reported 2,4-0 --I 9-J3-'17NT 973447 __ 2,4,5-TP (Silvex)
Dale Analy1.cd Lab Number --1)11...; l]I)] (llrvi~,·11 7/IJ\'\
1· ' ' N.C. Di:p:.irtmcnt of Environment,
I !callh, & Natural Resources
Solid ~astc Management Division
SAMPLE ANALYSIS REQUEST State Laboratory o[ Public Health
P.O. Box 28047, 306 ~-Wilmington Street
Jlalcigh, North Carolina 2761 I
•• ile Number_;_M_.::;c..:.;,o'-'-o--"'-~Z...."-----_s_S_5 _ _;_7_1'--Z... ___ Field Sample Number o·:z_p 3;z. __ s
Name of Site S(jmo/1 .5 sqzn 'c:... ]4;1 /c... Site Location Sf des 1/r l /e_
I Collected By 0-S, ID# ___ Date Collected B(-zs(c;1 Time __ (_3_c/S:,:__ __
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Resuits(mg/1)
I Environmental Concentrate Comments Arsenic --
Sect\ ·o\ e,\+ Barium --__ Ground water (1) _Solid (5) Cadmium --, Chromium
I P.20:J:eri)U'.\c1 $.±e0M --__ Surface water (2) _· Liquid (6) Lead --__ Mercury
V Soil (3) _ Sludge (1) ss-00-sD Selenium --I Silver --_. Other (4) _ Other (8) --
--. I --Organic Chemistry Inorganic Chemistry --
I Parnmctcr Results (mg/I) Parameter Resulls(mg/1) (mg/kg) Organic Compounds Results(mg/1)
VP&T:GC/MS Arsenic benzene : ----Acid:B/N Ext. Bariur.:i carbon tetrachloride ------MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------
--Coppe,· o-cresol
I ----
--Fluoride m-crcsol ----hon __ p-cresol ----Lead cresol ------I ----Manganese --1,4-dichlorobenzene
--Mercury 1,2-dichloroethane --
--Nitrate __ 1,1-dichloroethylene --
I --Selenium --2,4-dinilrotoluene
Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----
I ...... _ .. _ Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hcxachforoethanc ----__ Gross Alpha --Conductivity --methyl ethyl ketone
I Gross Beta TDS nitrobenzcne ------
TOC pentachlorophenol ----
----pyridine
I Microbiology ----tetrachloroethylene
--__ trichlorocthylene
Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol -----__ 2,4,6-trichlor6phenol
----__ vinyl chloride
endrin --lindane
I Date Received AUG 2 8 1997 eD Reported by --
--melhoxychlor
toxaphene --Oc,tc Extracted Dale Reported 2,4-D --
I 973448 __ 2,4;5-TP (Silvcx)
Dale Analy1.cd 0, --,;:!3-'Tl NT Lah Number --1)1 IS 31')] (!~cviscd 2/!Jl)
I , N.C. Department of Environment,
l lcallh, & Nalural Resources
' Solid W~stc Ma'nagcment Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 280-.n, 306 N. Wi!mington Street
RB\eigh, North Carolina 27611 wlc Number Ale[) 00 z.._ sss 71 z_ Field Sample Numbe.-O ""Z-0 3,Z'f-
Namc of Sile S(jrno/1 S 5<f1J'c..-ffi/t/C.. Site Location Sf des Vi/ /e_
I Collected By ])A~ JD# ___ Dale Collected 0('?0(1,)7 Time 0'34,_f
I Agency: Hazardous Waste Solid Waste Vs u pe rfun d TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I E11vironmcntal Concentrate Comm.en ts Arsenic --
S,<? Ji (Y\ {'I\ t-Barium --__ Ground water (1) _Solid (5; Cadmium ---, Chromium I Davi~~
,
e'.){\Q --__ Surface waler (2) _ Liquid (6) Lead --Mercury
'v Soil (3) S <;,-/ 0-SD --
I _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --
--I --Organic Chemistry Inorganic Chemistry --.
I Parameter Results(mg/1) Parameter Results (1ng/l) (mg/kg) Organic Compounds Results(mg/1)
VP&T:GC/MS Arsc.nic benzene ----Acid:R/N Ext. Bar,um carbon tetrachloride ----MTBE Cadmium chlordane ------
Chl0ride chlorobenzene ----·--Chi.omiurr, chloroform ------
I --Copper o-cresol ----
--Fhmride m-cresol ----
--Iron p-cresol ----
I --Lead cresol ----
----Manganese --I ,4-dichlorobenzene
Mercury 1,2-dichloroethane ------
--Nitrate __ 1,1-dichloroethylene
I --Selenium 2,4-dinit rotol uene ----Silver heplachlor ----
Radiochemistry Sulfates hcxachlorobenzene
I ----······-··-Zinc hexach lorobutadiene
Parameter ----Results (l'Ci/1) _pH hcxachlorocthane --__ Gross Alpha __ Conductivity · __ methyl ethyl ketone
I Gross Beta TDS nitrober,zcne ------TOC __ , pcntachlorophcnol --
----pyridine
Microbiology I --__ lelrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophcnol
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --
I AUG 2 8 199'7 'fJ{) Reported by
lindanc
Dale Received --. mclhoxychlor --
--toxaphcne
Dale Extracted Dale Reported 2,4-D
I 973449 --
Cf-,,B-9711d
_ 2,4,5-TP (Silvcx)
Dale AnalyrcJ Lab Number --1)11<..; 1.Jlll (1?,..vi,·,•d 1/(Jl\
, i'.C. Dcp;inn:cnt of Environment,
I I lcalth, & Nalur.il Resources
, ,' Solid V{3stc Ma-nagcmcnt Division
SAMPLE ANALYSIS REQUEST State l....&boratory of Public Health
P.O. Box 28047, 306 N. Wilming,on Street
Raleigh, North Carolina 27611
'?>.le Number A.lei) C'0 z_ ss.s 71 z... Field Sample Number D ·-z.,o s-Z5
I · Name of Site_S; ........ 13"1' _m.o;Oe.c/1-=.S=--~Y'f=F''--n_'..cc:...=--~Yac..=..c~/!_f~C. __ Site Location Sf .;Jes vr l le..... I Collected By j S ID# ___ Date Collected 0(--zep ( t/ 1 Time_-'-( ·cc.3o...c.· --'i)=----
Vsuperfund
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Agency: Hazardous Waste Solid Waste ----
Sample Type
Environmental Concentrate Comments
/)(r.l.. (,J ('1-<?.-di-IC~ __ Ground water (1) Solid (5) ·or s1iz. __ Surface water (2) _·_Liquid (6) St; .
V Soil (3) _ Sludge (7) SS-1 I -'::>L
_,Other (4) _· Other (8)
Organic Chemistry Inorganic Chemistry
Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg)
Vr&T:GC/MS --Anenic
Acid:B/N Ext. --Barium
MTBE Cadmium --Chloride ----Chrorcium ----
--__ Copper
Fluoride ----Iron ----Lead ----
----Manganese
----Mercury
Nitrate ----Selenium --Silver --Radiochemistry Sulfates --..... ·-··--· Zinc --Parameter Results (PCi/1) --pH
__ Gross Alpha __ Conductivity
Gross Beta TDS -· --TOC --
--Microbiology --
--Parameter . Results (Col/100111!) --
----
----
Date Received AUG 2 8 1997 eO Reported by
Dale Extracted Dale Reported
Dale Analysed 9 ".13-97 ,ij Lah Number 973450
DI IS )l1Jl (llr:vi~cu 2/91)
TCLP Compounds
Inorganic Compounds Resuits(mg/1)
Arsenic --Barium --Cadmium --Chromium --Lead --
--Mercury
Selenium --Silver --
----
--
--
Organic Compounds ResulLs(mg/1)
benzene --carbon tetrachloride --chlordane --chlorobenzene --chloroform --o-creso! I --m-cresoi --
--p-cresol
cresol -~
1,4-dichlorobenzene --1,2-dich loroethane
__ 1,1-dichloroethylene
2, 4-dinilrotoluene
__ heptachlor
hexachlorobenzene --hexachlorobutadiene --hexachloroethane --__ methyl ethyl ketone
nitrobcnzene --
--pentachlorophenol
--pyridine
tctrachloroethylene --• __ trichlorocthylene
__ 2,4,5-trichlorophenol
__ 2,4,6-trichloropheool
--vinyl chloride
endrin --iindane --methoxychlor --
--toxaphene
2,4-D --__ 2,4,5-TP (Silvex)
--'
N.C. D~panr'i1cnt of Environment,
l lt:a!th, & Natural Resources
Solid ~Vastc Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
.. ilc Number NCO D(; Z-SS5 71 Z... Field Sample Number __ ~oi~~~§_-1.Lll!.3.L~
... Name of Site SJ3rno/l s S<fkc... 7?<.;1/c.. Site Location S1cd-es Vil /e.__ I Collected By ':, le:-ID# ___ Dale Collected <a/z0 (q, Time ( 5 ::,,_s -------
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
Sample Type Inorganic Compounds Resuits(mg/i)
I Environmental Concentrate Comments Arsenic --
e:a c.-t+fj:lf".) u i\ cl
Barium --
__ Ground water (1) _ Solid (5) Cadmium --Chromium
I 1>,-c!,l(\lje., d,t'+eA --__ Surface water (2) _ Liquid (6) Lead --
J Soil (3) SS-1?, --s L-
__ Mercury
_ Sludge (7) Selenium
I --Silver --_ Other (4) _ Other (8) --
--
I --
Organic Chemistry Inorganic Chemistry --
I Parameter Results (mg/I) Parameter Results(mg/l)(mg/kg) Organic Compounds Kesults(mg/1)
V P&T:GC/MS Arsenic benzene ----
' _ Acid:B/N Ext. Barium carbon tetrachloride ----
MTBE Cadmi~m chlordane ------
Chloride chlorobenzene ------Chromium chloroform ------
I --__ Copper o•crcsol --
--Fluoride m•crcsol -----Iron p-cresol ------
Lead crcsol ------I --__ Manganese 1,4-dichlorobenzene --
--__ Mercury 1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylene --I Selenium 2,4-dinitrotoluene ----Silver __ heplachlor --
Radiochemistry Sulfates hexachlorobenzene ----
I ······-··-Zinc hexachlorobutadiene
Pa!'amctcr ----Results (PCi/1) pH hexachloroethane ----
__ Gross Alpha __ Conductivity methyl ethyl ketone --
I --Gross Bela TDS nitrubenzc.nc ----TOC __ penlachlorophenol --
----pyridine
I Microbiology --__ tetrachioroethylene
--__ trichloroethylene
Parameter· Results (Col/lOOml) __ 2,4,5-lrichlorophenol --
----__ 2,4,6-trichlorophcnol
----__ ,ioyl chloride
cndrin --lindane
I AUG 2 8 1997 B~ --Dale Rcccivccl Reported. by methoxychlor --toxa9hcnc --' D:itc Extracted Dale Reported 2,4-D --
I q -J..3-:17 -nd 973451 __ 2,4,5~TP (Silvex)
D,llc Analy1.cd Lab Number --l)llS Jl'JI (llcvis,;d 2/<Jl)
1-N.C. l)~partmcnl of Environment,
I !call~. & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laborntory of Public Health
P.O. Box 280-17, 306 N. Wilmington Street
Raleigh, North Carolina 27611
..,ile Number ;Ve,[) 00 2-SS5 7'f 2... Field Sample Number O ·-z_.o 527
Name of Site S,t3rno// ..S $qzkc.-7a,11/c.. Site Location SfdeJ VI/ /e_
I Collected By pA,:t JD# ___ Datc Collected s/z.s(07 Time _ __,(_'2,--=-,-z._-s __
I Agency: Hazardous Waste Solid Waste VSuperfund TCLP Compounds ----
Sample Type .Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
':::i"' ,l;/)\ e 1\ +-. Barium --__ Ground water (1) _ Solid (5) Cadmium --
I r{\_+. Chromium
StreNV\ --__ Surface water (2) _ Liquid (6) Lead --
ct ::,/\-;,_ --Mercury
\/ Soil (3) _ Sludge (7) r,,w..s--t-Selenium
I --Silver
_ Other (4) ,;.s.-I b/ Sb --_ Other (8) --
--I --Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) . Organic Compounds Results(mg/1)
~P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobcnzene ------Chromium chloroform ----
I --Copper 6-creso:-. ----
--Fluoride m•crcsol ----Iron p-cresoi ------Lead crcsol --I ----
----Manganese --1,4-d:chlorobenzene
Mercury 1,2-dichlorocthane -· ----
--Nitrate __ 1,1-dich!oroethylene --I Selenium 2,4-dinitrotoluene ----Silver heplachlor ----Radiochemistry Sulfates hexachlorobenzene ----
I ······-····-· Zinc hcxachlorobutadicnc
Parameter ----Results (PCi/1) _pH hcxachloroethane
__ Cross Alpha __ Conductivity __ methyl ethyl ketone
I --Cross Beta TDS nitrobcnzene ----TOC __ pcntachlorophcno! --
--pyridine --Microbiology I --_· _ tetrachloroethylene
--__ trichlorocthylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
--.. , . ·_. _l,4,6-trichlorophenol --
------vinyl chloride
. en<lrin --
{3i0 Reported by
lindanc
I Dale Received AUG 2 8 1997 --methoxychlor --
--loxaphcnc
Date Extracted Dale Reported 2,4-D
I 9 -;!.3-C/7 -n j
973452 2,4,5-TP (Silvcx)
Date Amtlyzcd Lab Number --I)! 1 '-1 \ IJ 1 { 11,.";~,·,l I/() 1 \
I N.C. Department or Environment,
I lcalt~, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 K Wilmington Street
R.eleigh, North Carolina 27611 wile Number NC./) a(; z.... sS5 71 z... Field Sample Number bc..,0 -~--z._"3
Name of Site SJ3mo/l S St:('·-h'c 7?!,/l/C.. Site Location Sfc,}--ey Vi //e... I Collected By JS ID# ___ Date Collected 'n{§ 11 Time /73'5
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
S:· J.t/Y\:?11-\-Barium --Cadmium __ Ground water (1) _Solid (5) --
I Wi l( io.MS ftl\ ci Chromium --__ Surface water (2) _ Liquid (6) Lead --
SS--17 -S. D --Mercury
l,r Soil. (3) _ Sludge (7) Selenium
I --Silver
_ Other (4) --_ Other (8) --
--I --
Organic Chemistry Inorganic Chemistry --
I Pura meter Results(mg/1) Parameter Results(mg/1) (m1:/kg) Organic CompGunds Results(mg/1)
VP&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbor. tetrnchloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chrorr,ium chloroform ------
I --Copper o-cresol -----Fluoride m-crcsol ------Iron p-cresol ------
Lead cresol --I ----
--__ Manganese --1,4-dichlorobenzcne
__ Mercury 1,2-dichlorocthane ----
--Nitrate __ 1,1-dichloroethylene --I Selenium 2,4-dinitrotoluene --Silver __ heptachlor --Radiochemistry · Sulfates hexachlorobenzene ----I ···•··-··-Zinc hexachlorobut adiene
Paramde_r ----
Results (PCi/1) pH hcxachloroethane ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Beta TDS nitrobenzcnc ----
TOC __ pcntachlorophcnol --
--pyridine --
I Microbiology --__ tetrachloroethylenc
--__ trichloroethylene
Parameter Results (Col/1001111) __ 2,4,5-trichlorophcnol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --
AUG 2 8 1997 {30 Reported by
lindane
I Date Received --
--melhoxychlor
--tox3phcnc
Dale Exl.raclcd Dale Reported 2,4-D
I Lab Number 973453 2,4,5-TP (Silvcx)
Dale Analyzed q -.;;i.3 J/7 71,;J --J)J IS J\1Jl (Rcvi.sr.d ?./9\).
I N.C. Dc-partmcnt of Environment,
I !call~. & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 2&¾7, 306 N. Wilmington Street
Raleigh, North Carolina 27611
.. itc Number lvcb C(; 2... sS5 71 z... Field Sample Number D --Z,0'?::,7_7
· Name of Site <y3mo/l S Stp-h'c 7?<.;1/c_ Site Location Sfdey 1/i //e_ I Collected By /rl L-ID# ___ Date Collected £cj-zrc,( <?1 Time / 1-45
I Agency: Ha,,ardous Waste Solid Waste V.superfund TCLP Compounds ----
Sample Type \norganic Compounds Results(mg/:)
I Environmental Concentrate Comments Arsenic --Barium _f_p1 7)1+ 11:-/ --__ Ground water (1) _ Solid (5) Cadmium
I --Chromium
I 0 -t," --__ Surface water (2) _ Liquid (6) Lead --Mercury
V Soil (3) S,<:, -!'3 -SL --Sludge (7) Selenium
I --Silver --Other ( 4) _ Other (8) --
--I --Organic Chemistry Inorganic Chemistry --
I Parnmcter Results(mg/1) Parameter Results (mg/l)(mg/kg) Organic Compounds Results(mg/1)
_lL:P&':':GC/MS ·Arsenic benzene · ----__ Acid:E/N Ext. Barium carbon tetrachloride ----
MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform . ------
I --Copper o-crcsol ----
--Fluoride m-cresol ----Iron p-cresol ------Lead crcso1 --I ----
----Manganese --1,4-dichlorobenzene
Mercury 1,2-dichlorocthane ----
--Nitrate __ 1,1-dichloroethylene --I Selenium 2,4-dinitrotol uene ----Silver heptachlor _ ----Radiochemistry Sulfates hexachlorobenzene ----I ······-·· Zinc hcxachlorobutadicne
Parameter-Results (PCi/1)
----pH hcxachlorocthanc ----__ Gross Alpha --Conductivity --methyl ethyl ketone
I. Gross Beta TDS nitrobenzenc ------
. TOC pcntachlorophcnol ----
----pyridine
I Microbiology --__ tctracnlorocthylcnc
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophcnol
----__ ,inyl chloride
endrin --
,BJ9P.cported by
lin<lanc
I Date Received AUG 2 8 1997 --methoxychlor --
--toxaphcnc
D:itc Extracted Date Reported 2,4-D --I q -.;>_4,q771j 973454 --2,4,5-TP (Silvcx)
Date Analy1.cd Lab Number --/)I !S 11 1Jl (!l.cvi.scd 2/911
I N.C. Oc.!pnrtment of Environment,
I lcalll), & Natural Resources
Solid Waste M'anagcmcnt Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
.. itc Number-'-AA--'--"'C::;.O'-----=D(;'-""--=2-'---=s;=-S-5=----7-'----'1-Z... ___ Field Sample Number O '?,,,o 3 "3.a
Name of Site S:Jrno/1 's St'fn'c 7?<.;1/c_ Site L-Ocation Sf des Vil /e__
I Collected By h 2'.-ID# Dale Collected 0/ 1J<.>( q] Time -----------
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
. Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --Barium
bpe1\ r /-::{I-·7.---
__ Ground water (1) _Solid (5) Cadmium --I Chromium
I o-bu --__ Surface water (2) _Liquid (6) . Lead --
V Soil (3) 5S-/l'f-Sl
__ Mercury
_ Sludge (7) Selenium
I --Silver
_ Other (4) --_ Other (8) --
--I --
Organic Chemistry Inorganic Chemistry --
I Purnmeter Results(mg/1) Parameter Results (mg/l)(mg/kg) Organic Compounds Results(mg/1)
VP&T:GC/MS Arsenic benzene ----Acid: B /N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Cl,loride · chlorobenzene ------Chromium chloroform ------
I --__ Copper o-cresol --
--fluoride m-cresol ----Iron p-crcsol ------
Lead cresol --I ----
--__ Manganese 1,4-dichlorobenzcne --
--__ Mercury 1,2-dichloroethane
--Nicrate __ 1,1-dichloroethylene --I Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --
Radiochemistry Sulfates hexachlorobenzene ----I ······-···· Zinc hexachlornbutadiene ----Parumctcr Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Bela TDS nitroben1..cnc ----
--TOC pcnlachlorophenol --
----pyridine
I Microbiology --__ tetrachloroethylcne
----trichloroethylene
Parameter Results (Col/lOOml} __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --
AUG 2 8 1997 i6~cporlcd by
lindanc
I D a I c R cccivcd
--__ mcthoxychlor
loxaphcnc --Date Extractcu Date Reported 2,4-D --I C/-Dif-9'711j 973455 __ 2,4,5-TP (Silvcx)
D"tc Anal,,cu Lab Number --1)1 IS Jl1JI mcvi~cd 2/IJJ)
' ' ' N.C. Department of Environment, I, 1.lc:ilth_, & Natural Resources
Solid \1/astc Mr.nagcmcnt Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilminr;ton Street
Raleigh, North Carolina 27611
-le Number /VC,Q Or';; Z-SS5 71, "L Field Sample Number b--Z.e.Y33 (
· Name of Site SJ3rno/l S 5t:fkc__ 7?!,/1./C. Site Location Sfq.fey Vi'( /e_
I Collected By /, 'Z..-ID# ___ Date Collected ~ z-'{ 1, Time { "f SO
I . Agency: Hazardous Waste Solid Waste VSuperfund TCLP Compounds ----
Sample Type iuorgal.ic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
~ Solid (5) Slu4f-/501'I Barium --__ Ground water (1) Cadmium --Chromium
I __ Surface water (2) pelo\AI /Cc:00!\ :t±3 --_ Liquid (6) Lead --J Mercury
S S----Z.. I -L,u .5 --_ Soil (3) V Sludge (7) Selenium --I Silver
_ Other (4) --_ Other (8) --
--
I --
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
V?&T:GC/MS Arsenic benzene ----Acid:b/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------. Chloride chlorobenzene ------Chromium chloroform ------
I --Copper o-cresol ----
--Fluoride m-crcsol ----Iron p-cresol ------Lead cresol ------I --__ Manganese 1, 4-di ch I oroben1.ene --
--__ Mercury 1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylene --
I Selenium 2,4-dinitrotoluene ----Silver hcptachlor ----Radiochemistry Sulfates hexachloroben1.ene ----
I ······-· Zinc hexachlorobutadiene
Paramrter ----Results (PCi/,1) _pH hexachloroethanc
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Bela TDS nitrobcnzenc --TOC __ pentachlorophenol --
--__ pyridine
I Microbiology --__ telrachloroethylene
--_. _ trichloroelhylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-lrichlorophenol
------vinyl chloride
endrin --
{tO Reported by
lindane
I 0;:itc Rccci·vcd AUG 2 8 1997 --melhoxychlor --toxaphcne --D"lc Extracted Date Reported 2,4-D --
I 9-JLJ-91r-rr-973456 _ 2,4,5-TP (Silvcx)
i),itc Analy,ed Lah Number --. 1)1 IS 31')1 (ltcviscd 2/91)
I N.C. DCpartmcnt of Environment,
I lcalth, & Natural Resources
Solid Waste M0anagcmcnt Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. llox 280J7, 3.:)6 N. Wilmington Street
Raleigh, North.Carolina 27611
.ilc Number-'-. M_c=i)'--CX;--"'-2... __ s_S_5 __ 7_C/,__2... __ _
Name of Site S(3rno// s Stpfi 'c... 72:{/l/c..
Field Sample Number C)'?,,Q)3,3Z--
Sitc Location Sfqj-ey I/(/ /e_
I Collected By f)/JJ ID# Dale Collected 0/1,1.p ( CF) Time Oq £,c,
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
S ( uc8 e /Sc, l/ Barium
~Solid (5)
--
__ Ground water (1) Cadmium --Chromium I pelow / .~5Dcr, -tts --
__ Surface water (2) _ Liquid (6) Lead --
SS --z.:z. -(,u S
__ Mercury
_Soil (3) V Sludge (7) Selenium
I --Silver
_ Other (4)
--
_ Other (8) --
--I .
--
Organic Chemistry Inorganic Chemistry --
I Parameter Results(rng/1) Parameter Resuits(mg/1) (mg/kg) Organic Compounds Results(mg/1)
VP&T:GC/MS Arsenic benz:!ne ----
Acid: B /N Ext. Barium carbon tetrachloride ----
MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------
I --__ Copper o-cresol --
--Fluoride m•crcsol ----
--Iron1 __ p-cresoi --Lead cresol
I ------
--__ Manganese 1,4-dichlorobenzcne --
Mercury 1,2-dichloroethane ------
--Nitrate · __ 1,1-dichloroethylene --I Selenium 2,4-dinitrotol uene ----
Silver __ heptachlor --
Radiochemistry Sulfates hexachlorobenzene ----
I ... , .. -.. Zinc h exa ch I orob 11 tad iene
Parameter ----Results (PCi/1) _pH hexachloroelhane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Bela TOS ni~robenz.cnc ----
TOC __ pcnlachlorophcnol --
--__ pyridine
I Microbiology --__ tclrachloroethylenc
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophcnol --
----__ 2,4,6-lrichlorophcnol
----__ vinyl chloride
endrin --
I AUG 2 8 1997 'f>f;) Reported by
lindanc
D,ttc Received
·--mclhoxychlor --__ toxaphenc
D:itc Extracted Dale Reported 2,4-0 --I C\-J4_cr7 I'll 973457 2,4,5-TP (Silvex)
Date Analyzed Lah Number --
1\11'-: "l.Hll (1),...,:,.,.,( 1/U1l
I ~.C. Dc!)Jrtmcnt of Environment,
, I lcalth, & Natural Resources
Solid \li'aslc Ma.nagcmcnt Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Ilox 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
.ile Number Alco D0 z_ s-S5 71 z._ Field Sample Number (!;)'-z.,,(:) 3,3 3
. Name of Site St3rno/1 S Sy?kc... 72uifc_ Sile Location Sf des VI l /e... I Collected By Sf::-ID# ___ Dale Collected Q,/Z1.p / q7 Timv L O'{---z__
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds ----
Sample Type lno~anic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --Barium
?·solid (5) Sf Jdc1e:-p;/e---
__ Ground water (1) Cadmium
J ) --Chromium
I a/' B/1 --
__ Surface water (2) _ Liquid (6) I -1 Lead --
SS-?.-3-W..5
__ Mercury
_ Soil (3) \,,Sludge (7) Selenium
I --Silver
_ Other (4)
--_ Other (8) --
--I --
Organic Chemistry Inorganic Chemistry --
I Pura meter Results(mg/1) Parameter Results(mg/1) (mg/kg) O~anlc Compounds Results(mg/1)
Vr&T:GC/MS Arsenic benzene ----
Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------
I --__ Copper o-cresol --
--Fluoride m-crcsol ----Iron p-cresol ------Lead cresol --I ----
--__ Manganese 1,4-dichlorobenzene --
--__ Mercury --1,2-dichlorocthane
Nitrate 1, 1-dichlorocthylene ------I Selenium 2,4-dinitrotol uene ----Silver heplachlor ----
Radiochemistry Sulfates hexachlorobenzene ----
I ······-····---Zinc hcxachlorobutadiene
Parameter ----Results (PCi/1) pH hcxachlorocthane ----
__ Gross Alpha --Conductivity . __ methyl ethyl ketone
I --Gross Bela TDS nitrobenzcnc --TOC _· _ pcnlachlorophenol --
----pyridine
I Microbiology --__ lelrachloroethylenc
----lrichlcroethylcne
Paramdcr Results (Col/l00ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --
(:fa lindanc
I Date Received
--
AUG 2 B 1997 Reported by methoxychlor --__ lor..aphene
Dale Extracted Dale Reported 2,4-D --I C(-,24-C/7-nd 973458 2,4,5-TP (Silvex)
Dale J\naly1.ed Lab Number --IHI'-ll!Jl (11,•vi~"'i 1/•ll\
. N.C. Dcp,;,tn;cnt of Environment,
I I lc..ilth, & Natural Resources
' Solid \_Vasle Mr.nagcmcnt Division
SAMPLE ANALYSIS REQUEST State l...aborawry of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Caroline. 27611
lktile Number A/C.,Q C(; 2..-SSS 71 Z... Field Sample Number 0~?, 31---
. Name of Sile S,3rno/lS Stpkc... 7?1.;1/c.. Site Location SfdeJ//i //e_ I Collected By 1~ -z, ID# ___ Dale Collected 0(-ze,, ( q 1 Time __ l__,_(-'-(-'g'-----
I Agency: Hazardous Waste Solid Waste Vs u pe rfun d TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
S{ uc/ei-e· ,,;/.,,_ Barium
~Solid (5)
--__ Ground water (1) Cadmium
j I --Chromium
I __ Surface water (2) f)eetf\. -z_ F'-f --_Liquid (6) Lead --' __ Mercury
_Soil (3) L,.r sludge (7) ss--z,r--Lu.$ Selenium --
I Silver
_ Other (4)
--
_ Other (8) --
--
I --
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Pa.rameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
_.k:::-P&T:GC/MS Arsenic benzene ----__ Acid:B/N Ext. Barium carbon tetrachloride ----
MTBE Cadmium chiordane ----
Chloride chlorobenzene ------Chromium chloroform ------
--__ Copper o-cresol
I --
--Fluoride m-crcsol ----Iron p-crcsol ------Lead crcsol ------I --__ Manganese 1,4-dichlorobenzene --
--__ Mercury 1,2-dichloroethane --
--Nitrate __ 1,1-dichloroethylene --
I Selenium 2,4-dinilrotol uene ----Silver heplachlor ----
Radiochemistry Sulfates hcxachlorobenzene ----
I ······-··--· Zinc hcxachlorobutadiene
Parameter ----Results (PCi/1) pH hcxachloroethane ----__ Gross Alpha __ Conductivity methyl ethyl ketone --
I Gross Beta TDS nitrobenzcnc ------TOC __ pentachlorophenol --
----pyridine
I Microbiology ----tetrachloroethylene
--__ trichlorocthylenc
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
cndrin --
AUG 2 8 1997 8P l:odane --
I Date Received Reported by __ melhoxychlor
--toxaphcnc .
Date l:xtractc<l Dale Reported 2,4-D --
I q-<JS-cr1 NI 973459 __ 2,4,5-TP (Silvcx)
Date Analyzed Lab Number
J)J IS )1 1Jl (!{cviscd 2/91) --
I N.C. Department of Environment,
, 1 !calth, & Natural Resources
Solid Waste Ma'nagcmcnt Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Ulrolina 27611
llllilc Number fv'c.,/) O(; 2-sss 71 z_ Field Sample Number ('.)'2--6?,?, s
· · Name of Sile S(5mo/l S 5:t'f·kc... 7a,/l/c.. Site Location Sf.qfey Vi/ /e...
I Collected By /,,..---z.._ ID# Date Collected 0(7(p (q7 Time /0 5° ------~---'----
I Agency: Hazardous Waste Solid Waste Vs uperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
~Solid (5) S( vdr:i.e Pile Barium --
__ Ground water (1) Cadmium --
I be,,,£ -(' . Chromium 3 ce+ --
__ Surface water (2) _ Liquid (6) Lead
u __ Mercury
_ Soil (3) V Sludge (7) 'SS---ZS --VJ-S Selenium
I --Silver --
_ Other (4) _ Other (8) --
--I --
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
VP&T:GC/MS Arsenic benzene ----
Acid:B/N Ext. Barium carbon tetrachloride ----
MTBE Cadmium chlordane ------
Chloride chlorobcnzcne ------Chromium chloroform ------
m --__ Copper o-crcsol --
--Fluoride m•crcsol ----Iron p-cresol ------Lead cresol --I ----
--__ Manganese --1,4-dichlorobcnzenc
__ Mercury 1,2-dichloroethane ----
Nitrate 1, 1-dichloroethylene ------I Selenium 2,4-dinitrotoluene ----Silver hcptachlor ----Radiochemistry Sulfates hexachlorobenzene ----I ······-"··-· Zinc hexachlorobutadiene
Parameter -----Results (PCi/1) pH hcxachlorocthanc ----__ Gross Alpha __ Conductivity __ mc:hyl ethyl ketone
I Gross Beta TDS ni~robcnzene ------TOC pcntachlorophenol ----
----pyridine
I Microbiology --__ tctrachloroethylcnc
----trichlorocthylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-1 richlorophenol
------vinyl chloride
endrin --
AUG 2 8 1997' #Reported by
lir.danc
I Date Received
--__ methoxychlor
__ toxaphcnc
Dale Extracted Date Reported 2,4-D --I q -a..'5-q, fJ', 973460 __ 2,4,5-TP (Silvcx)
Delle Analy-,cd Lab Number --' Ill!-; 11')1 (lfr·vis:cd 7/'Jll
II N.C. Dcp:inmcnt of Environment, g , I lca\\h; & Nal)Jral Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
.le Number NCO DC; Z-sS5 71 Z... Field Sample Number ____ o_·L--O __ :':>c:__3_1=. ______ _
Name of Site S-j:rno-'7.5 Yfn'r::...-Mille..
I Collected By j~ --Z-JD#
Site Location Sfq,./-es VI / /e_
Date Collected '?J{z.(; (q7 Time /osz
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
·':) u c{ c1 e, p1 /z_ Barium --
__ Ground water (1) ~ Solid (5) Cadmium
.J .I --
I Chromium I),; f' I I. c,Jr_ ' 3+-t. --
__ Surface water (2) _ Liquid (6) Lead
J ' --
S,::,-/"2-S -w~ __ Mercury
I _Soil (3). V Sludge (7) Selenium --Silver --
_ Other (4) _ Other (8) --
--I --
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
1/'P&T:GC/MS Arsenic benzene ----
Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------
D --__ Copper o-cresol --
--Fluoride m-crcsol ----Iron __ p-cresol ----
I --Lead cresol ----
--__ Manganese --1,4-dichlorobenzene
__ Mercury 1,2-dichloroethane ----
--Nitrate __ 1,1-dichloroethylene
I --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene
I ----...... -.. Zinc hexachlorobutadiene
Parameter ----
Results (PCi/1) _pH hcxachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Beta TDS nitrobcn1..cnc ----
TOC __ pentachlorophenol --· __ pyridine --
I Microbiology --__ tetrachloroethylene
--__ trichlorocthylcnc
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophcnol ---. __ 2,4,6-trichlorophenol --__ vinyl chloride --endrin --
I ~Reported by
lindane
Date Received _AUG 2 8 1997 --methoxychlor --__ toxaphene
Dale Extracted Date Reported 2,4-D
I --
/0-//i-9'172.,; 973461 __ 2,4,5-TI' (Silvcx)
Date An,tly-,ed Lab Number --,,,, . ~ ... ' "' ' ~ ,, . -
• • N.C. Department of Environment, D l lcallh, & Natural Resources
Solid Waste Management Division
. SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Uox 28047, 306 N. Wilmin&ton Street
Raleigh, North Ceroiil1a 27611
··le Number Ne)) 00 z_ sS5 71 L Field Sample Number ('.)(..,(:) 33,7
Name of Site SJ3rno// S Stjzkc 7??.;1/c. Site Location Sfq.}ey 1/1 //e_
I Collected By h -z__ ID# ___ Dale Collected ?:,(z_,i; ( 47 Time I ( 1-f
I
I
I
I
I
I
I
I
I I
Agency: Hazardous Waste --Solid Waste Vsuperfund
Sample Type
Environmental Concentrate Comments
__ Grnund water (1) _·_ Solid (5) Sor·/
__ Surface water (2) _._Liquid (6)
V Soil (3) _ Sludge (7)
_ Other.(4) _ Other (8)
Organic Chemistry
Parameter
VP&T:GC/MS
Acid:B/N Ext.
MTBE
Results (mg/I)
Radiochemistry
Parameter
__ Gross Alpha
Gross Beta
Results (PCi/1)
Microbiology
Parameter Results (Col/lOOml)
Inorganic Chemistry
Parameter Results(mg/l)(mg/kg)
Arsenic
Barium
Cadmium
Chloride
Chromium
__ Copper
Fluoride
Iron
Lead
__ Manganese
__ Mercury
Nitrate
Selenium
Silver
Sulfates
Zinc
pH
__ Conductivity
TDS
TOC
Date Received AUG 2 8 1997" R,IJ> Reported by ----------
D:lle Extracted _________ Dale Reroricd _______ _
Date 1\11;,lr,cd iO-/'f-C/] /JfI_ Lab Nurnbc-r ---973462
1)1 :s }!1)1 (11.cviscd 2/9i~
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
Organic Compounds
ben1.cne
carbon tetrachloride
chlordane
chlorobcnzene
chloroform
o-cresol
m•crcsol
p-cresol
cresol
1,4-dichlorobenzene
1,2-dichloroethane
Results(mg/1)
Results(mg/1)
-------
__ 1,1-dichloroethylene _____ _
2,4-dinitrotolucne
heptachlor
hexachlorobenzene
hexachlorobutadiene
hexachloroethanc
__ methyl ethyl ketone
nitrobenzcne
__ pentachlorophenol
__ prridine
__ tetrachloroethylene
__ trichloroethylene
__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol
--vinyl chloride
endrin
lindane
melhoxychlor
__ toxaphcne
2,4-0
__ 2,4,5-TP (Siivex)
------
------
------
I , r-:.C. Dc{rnrtmcnt of Environment,
, 1 \ca\th\ & Natural Resources
Solid Waste Ma'nagcment Division
SAMPLE ANALYSIS REQUEST
sS5 712-Field Sample Number
State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
o l.--0 3·3 B llltte Number Alco 00 z_
Sfde;sn l/e-Name of Site C..,' ( 5qz-kc ?a./l/c_ Site Location grno/lS
I Collected By Sf:'.-. ID# Date Collected
06(2 <,, {_ C{'l Time {/4-l
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds
----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
~r{~-z ce S.Dl I Barium --
__ Ground water (1) _ Solid (5) Cadmium --
I Chromium " +-·-tu --
__ Surface water (2) _ Liquid (6) O 1.Joce,-Lead --
V Soil (3) .:frog.., -r/l-,J:, *1 __ Mercury
I Sludge (T) Selenium --Silver
_ Other (4) SS -·z; -SL --
_ Other (8) --
I --
--
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
VP&T:GC/MS Arsenic benzene ----
Acid:B/N Ext. Barium carbon tetrachloride ----
MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------
I --__ Copper o-cresol --
--Fluoride m~cresol ----
--Iron __ p-cresol --
I --Lead cresol ----
--__ Manganese --1,4-dichlorobenzene
__ Mercury 1,2-dichloroethane ----
--Nitrate __ 1,1-dichloroethylene
I --Selenium 2,4-dinitrotoluene ----
Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene
I ----
······-·· Zinc hexachlorobutacliene
Parameter ----Results (PCi/1) pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Beta TDS nitrobcnzcnc ----TOC __ pentachlorophenol --
--__ pyridine
Microbiology I --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol ----
----__ vinyl chloride
endrin --
I eJ{cportcd by
!indanc
Date Received AUG 2 8 1997 __ methoxychlor
__ toxaphenc
Dale Extr'1clcd D'1tc Reported 2,4-D
I ---
973463
__ 2,4,5-TP (Silvcx)
[):i1c Analyzed '!0-i'-/-q7 /Jli.__ Lab Number --I \l ". "I 1' '1 Ill -.:., .. , ., /fl''
.
U' · N.C. Department of Environment,
I lcal!h, & Natural Resources
' Solid W~slc Mal'lagcmcnt Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. U_ox 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
.. le Numbcr-'-M-"'t:,""i)'----"-O(;--"'-Z-::.__S'--S_5_7-'--'C/_2...___ Field Sample Number ___ .....;b=-'Zo--''3,'-3"'-'-"J _____ _
. . Na me of Site_St.,,_lj,eir '-"rn.,.,o"-'/l_..:...:..5:...._~Yf='--1)-'-'-=c:....=---~Mc.=c.c/t..:c/<c__c.__ Site Location. _ _;Ss.,:_i::_'cd-cy=.,""-'(/','--'/'--'!..../L::/ e_=-----------1 Collected By S k.--ID# ___ Date Collected __ a_eyc__"Z._0_· _:_(_q_7 ____ Time __ t_2o_s __ _
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Envircmrnental Concentrate Comments Arsenic --
boeu,1 Bc""cQl'e,J--c.l.::_ Barium --
__ Ground waler (l) Solid (5) Cadmium --Chromium
I ~rt$ c-J-tZ,Jc;s. --__ Surface water (2) _ Liquid (6) Lead --
hptl, ::,-':) l ( z, ~/--__ Mercury
VSoil (3) _ Sludge (7) Selenium
I --Silver
S,S,-Z 'Q-S,L --
_ Other (4) _ Other (8) --
--I --
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
-.lL'.°P&T:GC/MS Arsenic benzene ----Acid: B /N Ext. Barium carbon tetrachloride ----
MTBE Cadmium chlordane ----Chloride chlorobenzene ------Chromium chloroform ------
I --__ Copper o-cresol --
--Fluoride m-crcsol ----Iron p-cresol ------Lead cresol .
I ------
--__ Manganese --1,4-dichlorobenzenc
__ Mercury 1,2-dichloroethane --
--Nitrate __ 1,1-dichloroethylene --Sel~nium I 2,4-dinitrotolucne ----Silver heplachlor ----Radiochemistry Sulfates hcxachlorobenzene ----I ... , .. _,, Zinc hexachlorobutadiene
Parameter ----Results (PCi/1) pH hexachloroelhane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
m
Cross Beta TDS nitrobenzcnc ------
--TOC pcnlachlorophenol --
----pyridine
n Microbiology ----tetrachloroelhylene
u --__ trichlorocthylene
Parameter Results (Col/l0Oml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
. endrin --
AUG 2 8 1997 {:f) Reported by .
lindane
E Date Rcccivccl --__ melhoxychlor
__ toxaphcnc
Dale Extracted Date Reported 2,4-D --I 10 -t'f-t71 I.fr 973464 __ 2,4,5-TP (Silvex)
Dale Analyzed Lab Number --l)J IS 3!1Jl (l{cviscd 219n
0 N.C. Dcpurtmcnt of Environment,
. I \calth1 & Natural Resources
Solid W-asle Mallagcment Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
.. le Number Alco Q;; Z-sS5 71 z... Field Sample Number o·-u::,34-D
Name of Site 51:Jmo// S $Lf-h'c.... 7?;11/c.. Site Location Sfq.}cy Vi'( /e....
I Collected By Sl-ID# Date Collected yzc,.; q·7 Time ('::,/7 -----------
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
'i7 . d So,/ Barium --
__ Ground water (1) Solid (5) ta C kj@! C\. · Cadmium --. --Chromium
I z ti --z., { b?r-M --
__ Surface water (2) _ Liquid (6) Lead --
SS-?.Cf-SL
__ Mercury
V Soil (3) _ Sludge (7) Selenium
I --Silver --
_ Other (4) _ Other (8) --
--I --
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
V P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium --carbon tetrachloride --MTBE Cadmium chlordane -----Chloride chlorobenzene ------Chromium chloroform ------
I --__ Copper o-cresol --
--Fluoride m•cresol ----Iron __ p-cresol ----Lead crcsol --I ----
--__ Manganese --1,4-dichlorobenzene
__ Mercury 1,2-dichlorocthane --
--Nitrate __ 1,1-dichloroethylene --I Selenium 2,4-dinitrotolucne ----Silver ' heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----n ..... ,-.. Zinc hexachlorobutadiene
Parameter ----. Results (PCi/1) pH hexachloroethane ----
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
~ --Gross Beta TDS nitrobenzcne ----
--TOC __ pcntachlorophcnol
----pyridine
I Microbiology --__ tetrachloroethylene
I --__ trichloroethylene
Parameter Results (Col/JOOml) __ 2,4,5-trichlorophenol --t.: --__ 2,4,6-trichlorophenol
----vinyl chloride
endrin --
{?:f) Reported by
lindanc
I Date Received AUG 2 8 1997 --methoxychlor --__ toxaphene
Dale Extracted Date Reported 2,4-D
I 10 -1'-1 -9? Afr 973465 __ 2,4,5-TP (Silvex)
Dale Analyzed Lab Number --!)I IS Jl'Jl (ltcvi.<:cd 2/91)
I , i',:.C. Department of Environment,
I lcalth, & Natural Resources
· Solid Waste MaTlagcmcnt Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public llca!th
P.O. !lox 28047, 3()6 N. Wilmington Street
Raleigh, North Carolina 27611
.. le Number~. M..:..scC:::.O<-.:::D(;'-"<-Z-=--....:S=-S-=5=---'-7-'C/'---2....=____ Field Sam pie Number 0 t.-0 ;£{-(
Name of Site c;,yrno/1 's Stp-kc..-72:ui/c. Site Location Sfqfey ville...
I Collected By Sf:--ID# ___ Date Collected 0/ U / <JJ Time ( 3, 37
I Agency: --Hazardous Waste Solid Waste Vsuperfund
Sample Type
n Environmental Concentrate
__ Ground water (1) _ Solid (5)
Comments
D __ Surface water (2) _Liquid (6)
D
V Soil (3) _ Sludge (7)
_ Other (4) _ Other (8)
Organic Chemistry Inorganic Chemistry
I Pnrnmeter
VP&T:GC/MS
Acid:B/N Ext.
Results(mg/1) Parameter Results(mg/J)(mg/kg}
Arsenic
Barium
I
I
MTBE
Radiochemistry
Parameter
__ Gross Alpha
Gross Beta
Results (PCi/1)
Microbiology
Results (Col/lOOml)
Cadmium
Chloride
Chromium
__ Copper
Fluoride
Iron
Lead
__ Manganese
__ Mercury
Nitrate
Selenium
Silver
Sulfates
Zinc
pH
Conductivity
TDS
TOC
I Date Received AUG 2 8 1997 ,{?:P Reported by _________ _
D:itc Extracted _________ Date Reportcd_--,------~--
1 1);1te Analy,:cd 10--14-91 NT Lab Number 97J4GG
I) I f<..; l 1 <! 1 ( ll rvi(r• ~rl~,~1,~117, -'---'-----'--'--------------
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-crcsol
p-cresol
cresol
1,4-dichlorobenzene
1,2-dichloroethane
Results(mg/1)
Results(mg/1)
------
-------
__ 1,1-dichloroethylene ______ _
2,4-dinitrotoluene
heplachlor
hexachlorobenzene
hexachlorobutadiene
hexachlorocthane
methyl ethyl ketone
nitrobcnzcne
__ pentachlorophenol
__ pyridine
tetrachloroethylene
trichloroethylene
__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol
vinyl chloride
cndrin
lindanc
__ methoxychlor
__ toxar,hcne
2,4-0
__ 2,4,5-TP (Silvex)
-------
-------
I . N.C. Dcinutmcnt of Environment,
. I !caHr., & Nat~ral Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
s;SS 712._ Field Sample Number
State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
()~34--z_ ..,le Number Ale[) a;; z_
Name of Sile C/ I S,Zkc::_ 72)_;1/c. Sile Location Sfdesvr lie.. -ljrl10/I S
I Collected By Ste ID# Date Collected 0o{Z-~(:f.l Time /4{o
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds -----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrdte Comments Arsenic --
Ba cl::1yr<;).>vl :':)t:, 1 ,, I Barium --
__ Ground water (1) _ Solid (5) Cadmium --
I Chromium t -z_ -A-. dcffl,\ --
__ Surface water (2) _ Liquid (6) Lead --
l/soil (3) ss;-·3,1 -s,L. __ Mercury
I _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --
--u --
Organic Chemistry Inorganic Chemistry --
D Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
\_,,,-P&T:GC/MS Arsenic benzene ----
Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------
E --__ Copper o-cresol --
--Fluoride m-cresol ----
--Iron __ p-cresol --
E --Lead cresol ----
--__ Manganese --1,4-dichlorobenzene
__ Mercury 1,2-dichloroethane ----
--Nitrate __ 1,1-dichloroethylene
I --Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene
I ----...... _.,_ Zinc hexachlorobutadiene
Parameter ----Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone
I --Gross Beta TDS nitroben1..cnc ----
TOC __ pentachlorophenol --
----pyridine
I Microbiology ----tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --1: __ 2,4,6-trichlorophenol --
--vinyl chloride --cndrin --
I AUG 2 8 '1997 &9-Rcportcd by
lindanc
Date Received --__ mcthoxychlor
toxaphcne --
Dale Extracled Date Reported 2,4-0
I --
I0-15...cr,JJT 973467 _ 2,4,5-Tl' (Silvcx)
Dale Analy1.ed · Lab Number --I\IPl''>Ht</t\." . ,,,,,,,
I l\'.C. Dcjmrtri\cnt of Environment,
. 1 !calth, & Natural Resources
Solid Was1c Mallagcmcnt Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington StrcC·t
Raleigh, North Carolina 27611
Nle Number---'M--'-'=r.,C-i)<-=C(;--=--=z_-s=-S--=5=---_:7_1,.__Z.. ___ Field Sample Number o-Z,0~-3
Name of Site SJ3mo/l S Stf-kc.... ffi/1 /c_ Site Location Sf qJey VI '( /e__
1-Collected By ___ ..,j,<cS=:..... _____ ID# ___ Date Collected ca/zs; (en Time__._/--''t'i"'--?.'_<;;. __ _
..
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
'S::' d I me"+ Barium --
__ Ground water (1) _ Solid (5) Cadmium --
I 13€/cv.J kr,:v1~rftJ\
Chromium --
__ Surface water (2) _ Liquid (6) Lead --
T-xx\cf
__ Mercury
I
V Soil (3) _ Sludge (7) Selenium --I Silver
_ Other (4) SS-t I(:;, -SIJ --
Other (8) --
--I --
Organic Chemistry Inorganic Chemistry --
I Pnramcter Results(mg/1) Parameter Results (mg/l)(mg/1<&) Organic Compounds Results(mg/1)
VP&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ----
MT3E Cadmium chlordane ------
Chloride chlorobenzene ------Chromium chloroform ------
I --__ Copper o-cresol --
--Fluoride m-crcsol ----
--Iron p-cresol ----Lead crcsol
I ------
--__ Manganese 1,4-dichlorobenzene --
--__ Mercury --1,2-dichloroethane
----Nitrate __ 1,1-dichloroethylene
I Selenium 2,4-dinitrotol uene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----I ······-····-· Zinc hexachlorobu tadiene
Parameter ----
Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Beta TDS nitrobenzcne ----
--TOC __ pcntachlorophenol
----pyridine
I Microbiology --__ tctraehloroethylcne
----triehlorocthylene
Parameter Resulls (Col/lOOml) __ 2,4,5-trichlorophcnol --
----__ 2,4,6-trichlorophenol
-----vinyl chloride
cndrin --
I AUG 2 8 1997 ~f;) lindane
Date Received --Reported by __ methoxyehlor
__ toxaphene
D:llc ExlrJclcLI Date Reported 2,4-0 --I 10-15-97ITT 973468. --2,4,5-TP (Silvcx)
D,llc Analy-,cd Lab Number --1)11"-11!)\ /l?rv\~,-.d ;,11/1\
I 'N.C. Dcflartmcnt of Environment,
I lcallr .. & Natural Resources
· Solid Waste Ma'nagcmcnt Division
SAMPLE ANALYSIS REQUEST State Labora1ory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
14Jitc Number Alco [)(oz._ s;S.5 7C/ Z... Field Sample Number 07,o31'{-
Name of Site SJ3rno/l S $qz-h 'c:... ffi/1 /c_ Site Location Sf cde.r /// //e___
I Collected By ])uJ ID# ___ Date Collected 'Y':i(2._1s:, ( t?; Time b1( u
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds -----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
Si u c[ge .5£t ,~ le-Barium --__ Groundwater (1) _ Solid (5) Cadmium --Chromium I l»§oo~ 11=--s --__ Surface water (2) _ Liquid (6) Lead --Mercury
_ Soil (3) V Sludge (7) \)t:{~ 10-(\ Pee+ --Selenium
I --Silver
_ Other (4) ~S-~S--~\JS --_ Other(8) --
--I --
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
VP&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------
I --. Copper o-cresol ----
--Fluoride m-crcsol --Iron __ p-cresol ----Lead cresol
I ------
----Manganese --1,4-dichlorobenzene
__ Mercury 1,2-dichloroethane --
--Nitrate _· _ 1,1-dichloroethylene
I --Selenium 2,4-dinitrotoluene --Silver __ heptachlor --Radiochemistry Sulfates hexachlorobcnzene ----I ······-·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity · . __ methyl ethyl ketone
I Gross Beta TDS nitrobenzenc ------TOC pentachlorophcnol ----
----pyridine
I Microbiology --__ tetrachloroethylene
--__ trichloroethylcne
Parameter Results (Col/JOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --
I AUG 2 S 1997 (3/9-Reported by
lindane
Date Received --methoxychlor --toxaphene --D:ilc Extracted Date Reported 2,4-D
I --
973469 --2,4,5-TP (Silvex)
D;,tc A11aly1,cd ID-/ '-t-'T7 N, Lab Number --IH!>.; 11<ll /1/r.,O,·,·d ?/<ll)
I ..
?~;? •; '?'• :.: .. · :?.!~:~E" , ~; · . . ,. .. _-:::£1:⇒}i!l~~J(1~~:~1~::..,: · ~"·:,:-· ·; -_.!;--: :",.,;~",:t:"~~,,,;~'1;.'/,,,,,.: ·-.'"'~~ -c-.--~-.. ;,e,"m"'::~,,,;~""•,""t"'~~,r""'~~t
STATE LABORATORY o.-PUBti:c BMi.m -.;·-
PO BOX 28047 -306 N. WILMINGTON ST • .'RALEl:Ga'Nc 27611
ORGANIC CHEMJ('.AL ANALYSIS
\
I PVRGEi!BU!: COMPOUNDS 'LAB NO q1 3'14/.Q q13441 Cfl3446 q7 3Lf'fl'.l C)73L/50
FIELD NO Joo;JI .;iD3~ ;J.03;>3 ~0.3J4 .ic.a:25
I COMPOUJVD TYPE ( 3 ) ( .3 ) (3 ) '('.j" ·i ( .3 )
r;1.,~~ 'pp b)f>Pl11 ~lv)ppm: -;;,__;,, !'Pin /4-L 'L•[Jrn (pp_~ppm C . . ,..
CHJ.OROMETIIANE JO 1 A .. ix . ' • J ' . I l I l I VINYL CHLORIDE /() .
BROMOIIETBAl'nl: ;;;J 0 .
0 CHLOROETHAl'fE 10
TRICBLOROFLUOROME'l'HAN'E JO ,j ' I 'I , I ,/
I ACETOR ,;i.o 440 :r,c-36C\ J,C... I I 6 :J',c., ;/31'.t, JjC... I 1 J,c..,
5 I l 1.1-DICHLOROETHEN!: (_,\_,, ll.-I I u_.
I JOOOIIETH.Altt I
KE'THTIZNE Clll.ORIDI!: I ' I
I CARBON DISULFtDI!: I +rcice
TRAl'l'S-1,2-DICHLOROETHER J, I l
ACK!LOlffl'RILE ;2.0
l, 1-DICBLOROICTHAl'fE 5
2-Btn' All'O!B .;10
I Cls-1,2-DICHLORO~HENE 5
CHLOROFORM
I 1,1.l•TRICHLOROE'l'IIAZU
CARBO!I TETRACHLORIDE
I BENZE!<E
l,l•DICHLOROETUAlfE
I TRICHLOROETH.ent
1.2-DICHLOROPROPANB
BROMODICHLOROIIETHANE ' I \I '\ I \ I \ / -JI I
I C-i'"'""''Sl.c I.II& co>ITl\~11,iffr\ON oR 8Ac.l,6~oui-t D, J -E■timated value
K -Actual value i ■
known to b• le■■ than value given. L -Actual value i ■ known to b• greater than T&lue given. O -Material wa■ analyxed for.but not detected. The number i■ the Kini.mum. Detection Limit. RA -·Hot analyzed. . . · 1/ -Tentative identification. ·
I !I -cc~po14plD Rei..! l'\eL'f OE.TI:cn•,s~ ON~ IN 111611 Cc,Na:NrRIITTOf'IS, ✓-SA.'IPLII. H16'+1L'f OILIATI.O, ,-iOL.'~ 00 NOT' APPLY,
•1'i :~ 3~:',(10/9~), ·, ' ', ': ;?;t:,,:;:.,ii\{;¥i{;~;~; '• };; '/; •, ,S, •,.i.·.·.'.'.· .. ,,i .. •.:;~~.~.•.'.-.·~.•.,,.'.:.t,;';:,~.;.1::~1.,f,·~~.•.•.:.t~ .... ·,: .. ·,·.:f.~;,:,~.;_~.•C:~.'~ .. ~;,,'..}l\,_~,;:.-:•.:,., '• .. ::.;::. ':),;}{~}jJ{?)\;;t<.'"t:, . > . -' .
C/73'-/6 /
;i.o3:'J&.,
( 3 )
'(jp_p} 1aim ·
I
" I
8-.:i,c_
11
, I
PtJRCCOM.ORG ........ ,. __ ,;,
•\:..:;.,,
''
I
I
8rATE LABORATORY OF PUBLIC HEALTH .. •
'
ORGANIC CHEMICAL ANALYSIS
PO BOX 28047 -306 N. WILMINGTON sr. RALEIGH. NC 27611
I
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f
I
r
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I
P!/RGEAIILE COMPOUNDS LAB NO 97344w q,3441 q73LJ Lf/3 CJ73L/lf9 19731-/50
FIELD NO I
COMPOUND TYPE ( 3) (..? ) ( 3 ) ( .3 ) I ( 3 )
~~S):, ~Pb ~ppm tPP.b)-,,p/tJ 'ppg} ppni_ fPP.b)p,pm iv,;M:,, ,r~~ r,m;
nmROMOHETHANE s ~ LL LL L,L I I l .
4-METHTL-2-PENTAKONE ,o \
CIS-l.3-DICHLOROPROP£NE 5 ' I ,/
TOLUElff: I :r -J. ( 11r"
11lAlfS.1,3-DICHLOROPROPER I , LL-
1.1.2,2-TETRACm.DROETllAl'flt
1, 1,2-TRICID.OROIC'J1L\lB \ /
2-IIEL\ffONE /0
T!:TRACHLOROE'nmR 5
DIBROKOCHLOROIIE'I'HAl'fE
ETHTI.ZlfE DIBROIIIDE I
I
CHLOROBENZDE I
l.1.l,2•n:I"RACHLOROETHAl'fE I
ETHYL BElfZEl'B .I
XTU:""8 I
STTREl{l!: ' I I
BROMOf'ORJI iO I
TRAffll-1,-1-DICHLOR0-2-BUTEl'B io I
1.l.3-TRICJn.OROPROPA!'fE ..5 I
1,"-DICBLOROBENZSNE I I
1,2-DtCBLOROBEZ'lZENE ,l,r I
1.l-DtBROM0·3-CHLOROPROPAl'fE ;iB I
I
VI1'fTL AC!:TATE ;wo "I ' I ' I ' I I 'I
Subs+;+u.+ed ben?on~ (J:)/r-J G G) (-} F) I GJ
4 /./ycfrocarl)of} ::> I
I
:
C -= P05518'-!;. l-l'IB O,l(TAl4 I~ f:rTIO N OR Bl=\ct;~OUJII O, .1· S11timated value
~ctual value i• known to b• le■a than 'ftlue given.
L -Actual value i■ known to b4I greater than value given. I
O' ... Jl&torial wa■ analped for but not detected. Th• number 1• th• Minimum Dat•ction Limit.
ID. -Hot analped. 'I 1/ -T•ntativ• id•ntification. , 'I.I -COMP<>llr-1D: R:ei.:.1AeJLY 1)61°1:c'f'ASU:. OIIJL'( JN J-fJ<rH coNCCN1RAT1otJ5, , ✓-SAl'IPLE H16-HLY [)ILuTED. MDL~ Do ..icn-APf'l-Y,
DEHNR 3068-0 (10/93) · • ,
cr,3'-f:51
( ::,; )
Vppb/pp"1
[)._...,
· .. ,
' /
G
PIJRGCOM.ORG ... j. :
''f'
, ·: ,.~ --~·· ·' il%f;_:tq'ft',''f"':Y'ty,fi~fAU ::;i' -,";.' ':/ : '-r~~!'€[£f;'.~~~{!~~~1f :r~: t. '. ?/(· · · ";;:1,-1'' · : · ,~;rf-f,:~!~:
STATE LABORATORY OF POBLIC BEALm
PO BOX 28047 -306 N. WILMINGTON ST . .'RALEIGII. NC 27611 ..
I PURGEABLE COMPOIINDS 'LAB NO
FIELD NO
ORGANIC CHEMICAL ANALYSIS
q734~ CJ13453 C)7.3'-l54
cJ.D3;J'7 .;2o.:U8 .xi:3;29
q73455 q73451o
c:20330 ,;2033(
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I
I
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I
I
It
I
I
COMPOOIVD TYPE ( .3 ) ( 3 ) ' ( 3 ) ( .:?, j' ( ·7 )
~~k)s C . KlPb)pprn_ l~b)pprn ~bypp1n ioPiyppm ppb)ppm
JO I • I J
. ., h . ' cm.oaoam-ntANE u..:,
VINYL CJD.ORIDE 10 -BROIIOIIETBAl'flC ;io
CBLOROETHAn 10
TRICBLOROFLO'OROICETHA!'fE JO '\ / ' , I
ACETOmi: ,;J_Q / 4 T,C. ,;:i,,;21.p;~ ;i_ :r,c.
5 1.1-0ICHLOROETHE!'fE LA--( A -I '
IODOlmTHAZ'fE
" laTHTU!:l'rE CHLORIDlt '
CARBOl'l DISULl'IDlt +rru~
TRAffS-1.l•DICHLOROETHErrE ,f I'
ACRTLOl<tTJULZ: ;;m
l, l ·DICBLOROK'l'HAl'fE 5
2-BOTAll'Ol'fE .;;10
CIS-1,2-DICHLOROETHJ!:NE 5
CBLOROJ'ORM
1,1,1-TRJCBLOROETHA!'I&
CARB01' TETRACHLORIDE
""""'""
1,2-DICBLOROETHAl'Ot
TRicm.oRO~
1.2-DICHLOROPROPAKE
BROMODICHLOROMETHAl'fE ' I \ I I I \ / .• \
.
c-ro:-,,;,a~ 1.#>e co.iT11"'11.i,rr10N oR BAc.l;.6Roui-&o. J -B■timat•d value
K -Actual value i• known to be l••• than value given.
L -Actual value i• known to be greater than value given.
U -Material was analyzed tor but not detected. The number i• the Minim.um. Detection Lim.it.
RA -Not analyzed. !/ -Tentative identification.
1/ • C01",Po1.11'D Ra.iAeL'f Oi<Tt:crl'l6L.f. OMCf '"' /Hui-I CelNC.£N~CV,,S. ✓-SA/IIPLC. H1'41L'1 DILl,.TEO, ,-IOL.'~ Do ~ ftPPLY,
DEHNR 3085-0 (10/9~!
; .\''.,:);:t: /~;.:;t-~ '·~--;·~· -
l.
.. t):p, :'trt_{· ~;~: .i>\.?" ·, ·,:, .
' . .,1.
, I
' ' soqr,c
I ,
" /
q73,.,57
ot033~
( 7 ) I
(3pJ:,. }a,rq
LL
' I + C.-,-etc e.
+v'()rP
LL
" I
+-.-,.,,.e_
I J
I
+race--
+,cue.,
-I-race
I I
J/
PORGCOM.ORG I I
I
I
I
I
I
I
I
I
I
f
m
111
0
I
I
. ·' --~ ,_ . -.·~ ·:f ''
i ;--
ORGANIC CHEMICAL ANALYSIS
PVRGEABU: CO.IIIPOVMJS LAB NO q72,45.] q73453
,, FIELDNO
CO.IIIPOVND TYPE l3l ( ..3 )
t 0f{' ,pi, ,ipp!Jl,,lppm {ppj);-ppttJ
DIBROIIOIIET1IAl'm 5 I LL,
4-METIITL-Z-PENTAl'l'ONlt -,o
CI8-t,S-DICHLOROPROPElfE 5 \ I
TOLUE?IE 3 j,C.,
TRAl'fS-1.3-DICHLOROPROPE.NE LL,
1.1,l.l-TETRACHLORO~ .
1.1,l--TRJCHLOROl:THAflE ,✓
2-HEXAl'IOHE JO
TETRACHLOROtrHER 5
DIBROMOCHLOROIO:THANE
ETHnZffE DIBROIIIDE
CHLOROBENZEl'JE
l, 1.1.l-TETRAClll.OROETHAl'lE
ETHYL BEl'IZEffE
XTU:ll'llS
srnun ,I
BROIIOFORII iO
TRAl'fS-l,4-DICHLOR0-2-BtrrER 'lo
1.2,S-TRICHLOROPROPANE ..5
1,4-DJCKLOROBEI'IZEKE I
t.:l-DICKLOROBENZEHE -!I
l,l•DIBROJIO-:S-CHLOROPROPANE ;i_E)
VfflTL ACETATE ;;i..()O \I , I
5,.wj-,'fu-1-«J brnrnnP:'S {1}/{) G) G
atUL t4tdroc.artx;n.:..
c-P~e~ 1..1"18 0,1'TRr,l.i~~j\ON OR BAa;6Rou1110.
J -l•timAt•d valu■
X -Actual value is known to be l••• than value giv■n.
L -Actual value is known to be gr■ater than valu■ giv■n.
9 -,34-54-q73455
.
(_3 ) ( ."3)
'ppJi) P('tf! fPPbJ,.p.pm
1 I -I l
'
\ I 'I
C:::J {"-)
</73'-IS(p
. ( '7 )
, . \), / ~Pi 'Prri;
I
\
,1/
...h--/)c.e.....
I 1
" I
+1~Qfl'-'_
I ' +,r /'I c_e_,
~3;:r
J
\ I
../--i,;,-,rP
I J
\ I
(+")
U -Material wa• anal~•d tor but not d■tect■d. Th• numb■r i■ th• Nini.mum. D■tection Limit.
IQ. -Not analysed.
1/ -Tentative identification.
11 -C:0MP01.ltJD. Rl:1.IFIEIL'f D6fEq".ffi31.E. C~L'( IN HIG-H ccr.JC(NlRAT10N."j,
✓ .-.s~_MJ'Lf. ,Hl6-H LY l)ILl.lTEO. MDL~ Do lllOT" ,Arri..'/.
DEHIIR 3068-0 (10/93) . , . ·· '.
; ·• .. ~~ ~~, /I'.:•':,, , '" i,,:';,,.
C/13'151
( ,; )
fppb ·r>P"J -,
\/
I / I
I I
,V
..J-.n1 c.e....
i I
\ f
I '7
11
J/ n
01
LL
' /
J;)f
lD
I ,
,, /
(+:
l'URGCOM.ORG
I
I
I
I
I
I
I
m
I
I
I
I
I
It
I
, .:~~{;•: . .,:?: ·-: -•·· . . ·; ·i·~·-.-_, '. ;y.·· .. -::f 0! t~~fill ltf ~~l~~:t~Wn~~;:::r ?-.•~ \ :.-·.--·:;{5tq~i:f::~-. ·_·,;:~ ~· .• _.;.
STATE LABORATORY OF_POBLIC HEALTH
PO BOX 28047 -306 N. WILMINGTON ST./RALEIGII. NC 27611
ORGANIC CBEMlCAL ANALYSIS
PVRGEAIILE CO!lfPOUNDS 'LAB NO q-,3 '+SB q7345q Q'134ci,O 9734w I q73tHo~
FIELD NO ;2D333 o1o334 c:20335 ,J.o 33((, ;;JD337
( 1 ) ' ,. (. r-r~i--~· . 1) ( :I ) ~ ) COllfPOUND TYPE : (
~~1;)5 C . 'ppb 1'('"1 AJb•pp,n /i;,bt,~pm /ot>b ilprn (ppb·km
Jo '-,-: ','i ;, ,./', Ti --CHLOROIIETBAlfE I -I / l_
VINYL CHLORIDE 10 .. -BROMOIU:l'HANlt ~o ...
CBLOROltT'HAN& 10
TRICBLOROFLUOROKETHAl'fE JO , ,I/ "\ I \I/ ' ' /
ACETQm,; .;2.0 60'-t :r;c 1 '7 :r;e, l.o :r,c.. / 0 :r,C-. i:;; :r,c...
1.1-DICBLORO&THEl'fE ;:= ,) u.... u_ I 1 u... I ,
JODOlif.ETH.Al'l'E I ._J,✓
laTHTLE?fK CHLORJD£ I \ I 9 :r,c.. \ V I
C.ARBOl'f DISULltD!; I 4 '.J ' ~Tnrf'_
TRAl'fS-1.2-DICID.OROETHEN'E J,, I I _ /,{
ACKTLOlm'RILlt ~ J,,
l, l•DICHLOROETllAlm 5 +r(lf'P
2.-BtrrAl'fOf'(E (MEKJ .;10 /O?Q._T
CIS-1.2-DICHLOROETHENE 5 + :f" sf
CHLOROFORM I i ../-ov.o
1,l,l•TRicm.0ROETHAl'fE I I;
CARBON TffRACBLORIDE {I \ / \ I ,I
Bl<!<ZEl<E ;).oo +,r,,,.,_ 35 Sr,,
1,2-DICBLOROURAR LL I J +(,JrQ. /;r
TRICHLOROE'l'llclm 3::r I
1.2-DICHLOROPROPAJIJE I ;__ -
BROMODICHLOROMETIIAN'E ' I .J1 ' I \ I \j ' j
c-P<>~l84> 4'& COl>ITF1"'1i,IR'1"10N
J -Kati.mated value oR BAc.l;.Ci~UJJ D.
X -Actual value ia known to be l••• than value given.
L -Actual value ia known to b• greater than value given.
U -Material••• analyzed for but not detected. Th• nu:m.ber i ■ th• Minimum. Detection Limit.
RA -Not analyzed.
1/ -Tentative identification.
'I,! -CO~ f'o141'lD RW Fl eL'( ·OETea'FI 61..E. O HU( 11'1 /II 6 II ec,Jc.E:/JT"Rf{r1cN5, ✓-~PLili. Hl~L'f C)ILU.TE.O, ,-\OL'~ Do NCr Ptf'PLy.
DEHNR 306&-0 (10/93). · · ·,;,;--,',;.;',,h\i; J,', • .
q-i_;; '-I &,.3
c2o33fl;
(3 )
7ppt, 1a>,rJ
u__.
·, I
' ··.;···,·. •,l :~-t.";c-.~' ~;' , 7·.~·,• ,·.:·,'.· ._,:\ .. J,;•,jl}";.'.l-~~;u--~1\,;;~~~,~~ii--""1~:',.•.,:·.-; .. I . . ·::· •, ,· ,.• -~.)::::✓,.,: .. :;i:t: : -~:,• ·~'.i:· .;. . '··-:,:~:" .-:· :.:~"' ·.;~;~~}-f~\·~;tfft••jt \.:.;:'".--~ .• ;· , _ -.4?\ ·t. ~~--•· -'. > ·,_❖:·: .. _~·~;·+.!~.~-j;t\?X?(t~·_._.·,
~/~) :~"~ ';i,~C.c'iil.f {'.'~Q~-.'. :: ~-'.~·;,7~••·•.~ :· ... ~,1~ff~rPf~1:~~"11~~t; ·
,:, .. ;,-;~ -., .. 1 •• : ~-' •• '
STATE LABORATORY OF POBLIC HEALTH
.. PO BOX 28047 -306 N. WILMINGTON ST •• RAimGH. NC 27611
ORGANIC CHEMICAL ANALYSIS
I
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P!IRGEABLE COMPOUNDS LAB NO q73J..j58 cr73459
., FIELD NO
COMPOUND tTYPE ( '7 ) ( '1 )
-~~~:, ti,pb),ppm 60.b. 1f-P/IJ
DmROMOllETHAlll!: 5 II / J
4-HETHTL-2-PENTAN'ONJ!: • ,o ,;J_;)__
Clfl..1,3-DICHLOROPROPENB 5 LL \/
TOLUEI'IE 1(o'74J' +rAce_.
TRANS-l,!S-DICHLOROPROP£NE I -I
l, 1,2,2· TI!:TRACHLOROrrHAN'E
-.J,7 I 1,1,:1-TRICHLOROE'TllAl'a . '
2-Hr.XAll'ONE JC .:J.J nd. :r
TETR.ACHLOROtrHENlt 5 '6'
DIBROMOCHLOROKETHANE I l.,L,
rm DraROMIDE J,,-\ /
CHLOROBE!'rZEfflt 1166-S-13
l,l,l,2·n:rRACHLOROETHAl'l'E I J I '
ETH1'l, BEl'IZZNE I ~34:r :J -s
:r:n.,;m,;s 3;03J 8
8TTRllE . I 11 -I
BROIIOFORM iO
TRAl'fS-1,4--DICHLORO-l-Btn'ENlt '60
1.2,3-TRICHLOROPROPAHE 5 i / ,/
1,4-DICHLOROBElfZENE I qqos 13
1,2•DICBLOROBEKZENE Ji ,1:2. 1
1,2-0IBROMO·S-CHI.,OROPROPAN'& ,9.E> IL-LL
VINYL ACETATE ;;;.(JO .J,; J,
fu.b:51-i +a.-led b en Zont:5 (£)/E) (-i-) (P)
{ Hydr;:Jcorbon5
c-1'<>"'518~ l..f'\B O>lffRt-lJNf\ilDl>I OR 5Acl;~ou1>10.
J -latimated valu•
K -Actual valu• i■ known to be l••• than value given.
97 3'-llo0 q73y CJ/ q ,J'/-1.t,;)
( 1 ) ( '7 ) L "", J
/ib· PP · Pptf! (ppbJp.pm /aiplJpm;
--I I . LL I I
\
' / 'V
yy,-:S" ~30°
I , / L-
' ,
-/-rr1c_P
I I
, ' I .I,
q7;;)__ J q 5 I :r I -c..
7 .,, E',
l..L L,._ I I
103 145 --J.-v-nrn C...
4wln -r '/ JO -:r -l--rn rn
c.,
fl I I
\ / \/ , I
JPJ/n J 331 .:r ;i s,c..,
:J.O 3if I
LL I
J, 'I ,v
(+J (-r {-+) \c -i~vel
L -Actual value i ■ known to be greater than value given.
O -Material wa■ analyaed tor but not detected. Th• number i ■ th• Minimum Dotaction Lim.it.
1/ -Tentative identification. I lilA. -Not analysed.
1, -COMPoU.t,ID. Rl:L-IAEILY P6TecrA0Ue. ()1\11..'( '"' HIG-H ccNCCN1RATJON5,
q,3'+lo3
I ,3 l
lppb PPIJJ
I I ,
' I
...L,,_,..,.,, "-
I
. ' /_
C)
. '
l ·'
... ,,/ c,~AMPl.;E t-116:~LY l)IL-LtTED, .MDL~ DO ~:APPL'/, . . . · .. : · . , . . ...
1,:: ~~~,~~u~,~~> , __ .. "I,:, ?·:o:· _:;};:~i'f~' '"';·;.,,,,,;':, :::,\}/L: . ·}::·;;ti~:i;i{l\\f~!:·:,~;~ii1
-~-~\ :=~\:~~.,1~.p.r ·r..: ._.: :, .. ,,.:-_ "· '.
I ' r ';;•· :;A·:.":' .. '...-ef'
I
ORGANIC CHEMICAL ANALYSIS
I PVRGEAIILE COMPOUNDS .LAB NO 913'-fl_.,y q73'1w'5 q t 3 'il,;,ls, C!73'-lw7 9 '7 341o6
FIELD NO ;;i.o 33 cf ;w340 -203 '-I I ,.;2.03'-};t '10 3'-/.3
CO.MPOVM> TYPE . ( 3) ( :3 ) ( 3 ) (3 ) (...;?) I ~~:, rpp,~l Pf'IT1 ~-b~ppm. 1,pi,\)J)/7/n /opb,!?pm l/ppb him · C .
:;J.O :-,,-, '-----' --'-../11 -CHLOROMETJLVQ: I ,·, I I I J I VINYL CHLORIDE 10 .
BROMOIIETBANE .::io
I CHLOROETHANE 10
TRICHLOROFLUORO.ll:E1'JlAlfE ,o ' I ' I ,I/ ' I , I
I ACETONE ;zo ;z s,c... ,:;)_ J,C.. 0%3}-ct;;i_ J,C. 43:s/-
1.1-DICHLOROETHENE ;;:: I I I...<--LG J I J -I 1
I IOOOJU:rHAlfE I
lmTHTIZB CHLORIDE I
' I CARBOJ'f DISULl'ID& I
TRAN'S-l,:l·DICHLOR0£THEB J,
ACRTLOlm"RILz: ;;iv
1, 1-DICHLOROE'I'BAl'(E 5
2-BOTAl'fOim .;10
I CIS-l,:l•D1Cm..0ROETHENE 5
Cm..0ROFORII
I l, l.1-TlllCHLOROETHA.lm
CARBOJ'f T!:TRACm..0RIDE
I BElttl:1"'
l,2•DICHLORO.ETHA10:
TRICHLORO~ I l,:l·D1Cm..0ROPROP.Al'm
BROMODICm..0ROIIETH.A.lm ' / ·, I \ / "' \ I ' I
I
I C -f'o:;,;, e~ ~ I> .::o.n-11~,p,1 AnoN oR 8Ac.t:;.6~oui-A D. J -Batimated value
X -Actual va.l.ue is known to be leaa than value given.
L -Actual value i• known to be greater than value given. ~
I
O -Material waa analyzed for but not detected. 'l'he number ia the Minim.um Detection Limit.
RA -Yet analyzed.
I
1/ -Tentative identification.
It -co,...po1,1p&0 Rw f'lel..'f ·OloTECT1181.£. OM&:,( IN IH6H CC1111c£,Jm,mc:N5, ✓-SAl'IPL6. H1'41L'f OILllTE.O, '401!~ 00 ~ Ptf'f>LY,
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PIJROCOM.ORO -•-.•:·J:
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•• .· 8rATE LABORATORY OF POBLIC HEALTH
PO BOX 28047 -306 N. WILMINGTON sr .. RAIEIGH. NC 27611
ORGANIC CHEMICAL ANALYSIS
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PVRGE/lBlE COllfPOVNDS LAB NO 9731.J.&iY· 9134t.,5
, , FIELD NO
COllfPOOND TYPE ( '2>1 ( 31
~Wf/ ,,. ppb ,ppm (ppb.JP-PlfJ
5 -'-./
omROMOllET1L\l'(E I J -11 -
4-METHYL-2-PENTAN'OrfE -,o
CIS,,,1,3-DICHLOROPROPENE 5
TOLtml'fE
TRANS-1,3-DICHLOROPROPENE
l,l,2,2·TETRACHLOROnHA1t'E
. ,v 1,1,2-TRICHLOROETHAN'E
2-HE.%.AlfON'E iC
TETR.ACHLORO.!:I"HE?ra 5
DIBROMOCHLOROKrrHANE I
l'fE DrnROMIDp; , I
CHLOROBENZElf!: -!-rnrP
1.1, l,2-TETRACHLOROETHAl'IE Ii
ETHYL BE?'IZEN'E J/
:nu:,n,:s lrf\rp c.,.
8TTRENl': ,/ J
BROKOFORM ;o
TRAlfB-l.4-DICHLOR0-2-Btn"E?fE io
1.2.S-TRICHLOROPROPANE 5 ,
1,4--DJCHLOROBEl'IZENE I + ,,-flrl°
(!_
1,2-DtCHLOROBENZENE ,Lt I 1
1.2-DIBROM0-3-CHLOROPROPANE ~c) i
VINTI. ACETATE ;J.()0 ,11 " /
Su bE,+i'hxhrl ben V n.o5 (±)/{-) B A
f, liyclt'Ocan'.lon5
c-l"0"518L{'_ L.l'IB O>IITAl'-l.l"'fl110M OR Bl\ct;~our-io.
J -Kati.mated value
~ -Actual value ia known to be le■■ than value giv•n.
L -Actual value i• known to bo greater than value given.
C/13'-flo~ q73L/lt>l q7341o8
J-.3 l ( 31 ' ( 3 l
!Pi b i fl >;}pp,(! /'ppb)p,p,ri ({Pti.ppm;
-
(A_, fl , /J
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C) (-(-)
U -Katorial ••• ana.l~od tor but not detected. Th• number i• tho Minimum Detection Limit.
ID. -Not analysed.
I 1/ -Tentative identification.
It -cOMPou.r,10.1tr;1..1Ae1..y P6iECff\-0LE. a/\lL'( ;N t-11~H co,,1ccN11<Ar10~.:;.
✓-SRl'lPLE H16-_HLY OILIATED, MDL~ Do~ APPJ..'/, · .. ,
DEBNR3088-0(10/93l ···'*'.' .,,,. ',·:•,···:,. . . , ' , .. .,,,.,, .. ,: ",,: I I \•}_;/;),,;,' ,\\;jJl;' ,_ .. , ·. . ,::' .. ' , 'I;.\i~:-:~:.,:)t:·::~·." .,-
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, l'URGCOM.ORG : .. •
NCDEHNR I ,, ·. Oi,;iSi•on of Waste Management
_M-. Superfirnd ·Section
Organics Lab: L--
Inorg;rnics Lab: --
□ Hazardous Waste Section _ It □ Solid Waste Section
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CHAIN OF CUSTODY RECORD
Project Name: S13mo115 ~(D'c 7zu1lc-
Site ID # (NCD#) N c../) ct, Z-5s; 7q Z-
Location: S'iAf-e;,1,/ !((_ /Ve
Address: l"U;;'c &fut,,-'--fZ_d.
Soil l,, \Vater
Sampled By: Dc,,1f'A-{JJr/.,,oyt
Sampler ID __________ _
Telephone:(fil) 7 33-7/'?io/ -qd-
Date Sampled: 'B/zs/11, eo/u(q1
~ . Time Sampled:
Waste L--Other
317
Sample Types: ------
ind, 'c,,.,fes ~~ fR__ f, u.S.1r-i'o,J r I? f /de ,i I,' ·
1 l tfJ'-c( w,H '1e
Field Sample °'-1D 3<(..S
Numbers o<.,() '3,. <;. z_
fco-zess5.
b '2JD "3,(_(,,
Relinquished By:
Received By:
(Signature)
Relinquished By:
Si nature
Received By:
(Signature)
Relinquished By:
Si nature
Received By:
Do uld <Z-a..r-t d f:-
o7..o ?:?(b 0'2o "'3-f, 07,o 'YfCo c:,zo:yf_Cj
o'ZvsS:.s o'Zc'.3.S:1= ~'<-<03.s.S ~E?b~
"i5t.C>°¼{) 07-6~( Dt-()~2 D703,63,
b '2<!:,:?,f, 7 ~c,2£:>-U,O
o<w ~ O'Z,<o-3,"> I
¥o-zo~l ~oZ<D ~8
c,,_c,·¥1-0--Zt> '¼$'
Time: (Qv
Date:t; W t/7 Time:/ D lo
Date: Time: --------
Date: Time:
Date: Time: ----
Date: Time: --------
'I
I ,· ;::,::c. D;:p'.i_rtmcnl of E1.wironmcnt, SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
I \cahh, & Natural Resources P.O. Box 2;8047, 306 N. Wiimington Street
. So\id ~'~'aslc Managem~nt Division Raleigh, North Carolina 27611
!La: ; ' I' ,v '7 --s 707 /h·'7, Q~_C.E\V_ ED -Sile Number 1v'C,u vro c..-f;:::, 1 '-Field Sample Number ___ ~I.J=-'-'~0 ___ ~ ~~!!f~--------
Name of Sile S(jrno/1 S . $qfi'c__ 7a,/l/C. Sile Location _ _,,_S._i_'cy-es-.:..=,_..,//'C--'.r-'-/_,_/e...=-_O_C_T_0_3_19_9---'7 __ _
I Collected By j .5 ID# ___ Date Collected_Cz?;~/--2.S~(~q~7--~S,-l.,,,.IP~E~RFtlhlT<l s~12~,
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Agency: Hazardous Waste Solid Waste Vsuperfund
Sample Type
Environmental Concentrate Comments
__ Ground water (1) _Solid (5)
__ Surface water (2) _ Liquid (6)
i./ Soil (3) _ Sludge (1)
_ Other (4) Other (8)
Organic Chemistry
Parameter Results(mg/1)
__ P&T:GC/MS
V Ac;d:13/N Ext.
MTI3E
--k 'f C/3 __ < o. Io fll"'
Radiochemistry
Inorga_nic Chemistry
Parameter
Arse:iic
Barium
Cadmium
Chloride
Chromium
__ Copper
Fluoride
Iron
Results (mg/I) (mg/kg)
Lead
Manganese
Mercury
Nitrate
Selenium
Silver
Sulfates
Zinc
Parameter Results (PCi/1) pH
__ Gross Alpha
Gross Beta
Microbiology
Paramckr Results (Col/lOOml)
l'QJ
Date Analyzed 9-1.1-97/(P
l)l!S .11'J1 {ltcvi~cd ?Nil
__ Conductivity
TDS
TOC
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
OrgijnJc Compounds
benzene
carbon tclra..:hioride
chlordane
chlornbenzcnc
chloroform
o-cresol
rr: •crcso:
p-cresol
crcsol
1,4-dichlorobcnzenc
--1,2-dichlorocthane
Resu(ts(mg/1)
Results(mg/1)
---
-------
__ 1,1-dichlorocthylene _____ _
2,4-dinitrotol uene
heptachlor
hcxachlorobcnzene
hcxachlorobu t adicnc
hcxachlorocthane
__ methyl ethyl ketone
nitrobcnzcnc
__ pentachlorophcnol
pyridine
tctrachloroethylcne
__ trichl<Y.octhylenc
__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophcnol
vinyl chloride
endrin
lindanc
mcthoxychlor
taxar,hcnc
2)4-0
------
.l,.l,.S.,1i,45ilvcx) /:J '11 _/~r;o-,.-,,_,__~~~f-9--3--
I _.N;C. Dc~J,ar:rncnt of Environment,
I lcallh, & Natural Rcso,Hccs
, Solid ~'-aslc M:.nagcmcnt Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolin• 27611
... ilc N um ber-'M---'--'=t:.."'u"--'Oe;=-""---=z__:..__...:s:.._s__.c:5:..__..:.7-'1'--z...___ Field Sam pie Number b .. ?..0 3-f{,
-Name of Sile S,,3mo~ s sq:,n·c 7a,/l/c.. Sile Location Sides 1/r l /e__ I CoHccled By j S ID#~~-Dale Collected ,e(z..s( q1 Time /'f-10
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
-Sample Type Inorganic ·Compounds Resul(s(mg/:)
I E11vironmcntal Concentrate Comments Arsenic --
2:>e,~ime~+-, 6o. ck-<a µN\
Barium --
__ Ground water (1) _ Solid (5) Cadmium --,
Chromium I 'D0'\Cl --
__ Surface waler (2) _ Liquid (6) Lead --I Mercury
":::/;,, .. C> '6 -S, t) --
I JL.. Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) __ Other (8\ --
--I --
Organic Chemistry Inorganic Chemistry --
I· Puramc!er Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Rrsults(mg/:).
_ 1'&':':GC/MS ' Arsenic benzene I ----
Acid:13/N Ext. Barium carbon tetrachloride ----MTSE Cad'mium · chlordane --KB ----
...J::::. <0,/0 {¥-tll Chloride chlorobenzene ----Chromium chloroform ------
I --Copper o-crcsol ----
---Flu0ridc m~crcsol ----Iro,. p-cresol ------Lead crcsol I -.-. ----
----Manganese --:,4-dichlorobcnzene
--. Mercury 1,2-dichloroethane ----
--Nitrate __ 1,1-dichloroethylcne
I --
) Selenium . 2,4-dinilrololucne ----Silver __ heplachlor --Radiochemistry Sulfates hexachlorobcnzene ----I ······-·· Zinc hexachlorobutadiene
Parametei-----Results (PCi/1) _pH hexachloroelhanc
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I ·--Gross Beta TDS nitrobenz.cne ----TOC __ penlachloropl,enoi --
----pyridine
I Microbiology --__ lelrachloroelhylene
--__ lrichloroclhylene
Parameter Results (Col/1001111) __ 2,4,5-lrichlorophenol --
----__ 2,4,6-trichJorophenol
----__ vinyl chloride
endrin --
AUG 2 8 1397 BJ)Rcporled by
lindanc I Dale Received --
--methoxychlor
6f,.,14 ,, _ :7-411:'.t.-toxaphene --D:itc Extractcd(/'CIJ~-1f-?7V/J Date Reported 2,4-D
I (J,v,t --
Dale Analy1.cd~-ll--'l,ZJ/.P
973471 _ 2,4,5-TP (Silvex)
9-Y-!liLab Number
/)I !S .1l 1JI fl?.c.vi...:cd 7./911 --
N.C. Dcp..irtmcnt of Environment, I ' · 1 !caltt( & Natura! Resources
, Solid Waste M,anagement Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. I3ox 28047, 306 l\. Wilmington Street
Raleigh, North Ca~lina 27611
wile Number--'.M_c.=..co_~--=-z..._s_S_5_7__,_1_2-__ _ Field Sample Number 0.7-b 3 Cf.-7
Site Location SfcJ-es VI'( /e_ Name of Site S(_5rno/l·S Stpfi'c 72!.;1/c.. I Collected By ~ _<;, ID# ___ Date Collected f'.:fz S ( "'i I Time [ ·31.5 ----=---
I Agency: Hazardous Waste Solid Waste VSuperfund TCLP Compounds ----
Sample Type Iriorganic Compounds Resuits(mg/1)
I Environmental Concentrate Comments Arsenic --
SeJ1 ·1'1\ e.,\+ Barium --__ Groundwater (1) _Solid (5) Cadmium --
I P)t.t ck: §1vu"-d ~* <'ti',{\'\
Chromium --__ Surface water (2) _ Liquid (6) Lead --
ss-00-sb --Mercury
V Soil (3) _ Sludge (7) Selenium
I --Silver
_ Other (4) _·_ Other (8) --
--
--.
I --Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
_· P&T:GC/MS ', Arsenic benzene ----V Acid:B/N Ext. Bariuc:i carbon tetrachloride ----MTIJE Cad•mium chlordane --PU3 ----
..LL <:o, IOpp.r>t Chloride chlorobenzene ----Chromium chloroform ------
I --Coppe:-o-cresol ----
--Fluoride m-crcsol ----lion p-cresol ------Lead crcsol --I ----
----Manganese --1,4-dichlorobenzene
Mercury 1,2-dichloroethane ------
--Nitrate __ 1,1-dichloroethylene --I Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----
I ······-·· Zinc hexachlorobutadiene
Parameter Results (PCi/1)
----pH hexachloroethane ----__ Gross Alpha _· _ Conductivity --methyl ethyl ketone
I Gross Bela TDS nitrobenzcne ------TOC __ penlachlorophenol --
----pyridine
I Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/1001111) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --
{3 t[) Reported by
lindane
I Date Received AUG 2 8 1997 --
--methoxychlor
P;,fl..f,. Of,(,t/'7 ((I{._, toxaphene --D:ite Extracic,~ '1-8._-'l.7Jl,o Date Reported --2,4-D
I µ ' 973472 2,4,5-TP (Silvex)
Date Analy1.cd~'l-LL-~zu, 9•1~Lab Number
Ill IS Jl'JI (IZcviscd 2/91) --
I .. N .. C. Ocp.nr_tmcnl of Environment,
1 lcallh, & Natural Resources
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 280.n, 306 N. Wi!mington Street
Raleigh, North Carolina 27611 , Solid \~hslc M;,nagcmcnl Division
.. ile Number /VC,/) O(; Z... SSS 7C/ 2... Field Sample Numbe; (')"Z..OYfR
Site Location Sfq}ey(/( //e_ · Name of Site 5J3rno/l S Stjzfi'c 7?<.;,./c.
I Collected By hA0, ID# ___ Date Collected 'B(rz 0(cn Time OZ:,4'5' ---~---
I Agency: Hazardous Waste Solid Waste Vs u pc rfun d TCLP Compounds ----
Sample Type Inoiganic Compounds Results(mg/1)
I Environmental Concentrate · Comments Arsenic --
s,.., Ji fY\ Pl\ t Barium --__ Ground water (1) _ Solid (5; Cadmium --' Chromium I b a.v tr.f.~""
;
p>f\cf --__ · Surface waler (2) _ Liquid (6) Lead --Mercury
V Soil(3) SS.-(o--SD --
I _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --
I --
--
Organic Chemistry . Inorganic Chemistry --
I Parameter Rcsults(mg/1) Parameter Results (1ng/l)(mg/kg) Organic Compounds Results(mg/1)
_ P&T:GC/MS Ars.:.nic benzene --Bar;~m --V Acid:B/N Ext. I carbon tetrachloride ----MTBE Cadmium chlordane --Pc/3 ----V < o. Io l'/2-"'--Chhride chlorobenzene -----Ch,omiurr, chloroform ------
I --Copper o-cresol ----
--Fiuoridc m-crcsol ----Iron p-cresol ------
I --Lead cresol ----
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dichlornethane
--Nitrate 1, 1-dichloroethylene
I ----Selenium 2,4-dinilrotol uene ----Silver heplachlor ----
Radiochemistry Sulfates hexachlorobenzene
I ----..... ,_., Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone
I Gross Bela TDS nitrober,zene ------TOC __ pcnlachlorophenol --
--__ pyridine
I Microbiology ----telrachloroethylene
--__ trichloroethylene
Pam meter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --
I AUG 2 8 m7 e,iDRcportcd by
lindanc
_Date Received --methoxychlor /9-A '/, §47 --/4L. loxaphene --Date Extracted fl"B ?-?·'17 yt' Date Reported --2,4-D
I /3.u,t 9-17-? JIJf) 973473 __ 2,4,5-TP (Silvex)
Date Analy1.edf?Ceq,-t.L='17VP Lab Number --l}J IS 11!)1 (Hrvi .. rd 1/(/1\
~.C. Department of Environment, I '· ·1 lea 1th;
0&· Natural Resources
·, Solid Waste M~nagcmcnt Division
SAMPLE ANALYSIS REQUEST State L.&boratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
RB!cigh, North Carolina 27611
.. itc Numbcr-'Ni--'--"t:.,"'/)'----=Q;:;--=--.:...z.__s"--S---'5:....---'-7---'1'---Z... ___ Field Sample Number O 'Z..0'3f/--9
Name of Site <y3rno/l S 5:t'fkc 7Z:,./!/c_ Site Location Sfqfey VI/ /e_. I Collected By j S ID# ___ Date Collected 9( 7-(p ( t/ 1 Time_..i.{-=-3,o=-=-· ,:ell:.._ __
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
Sample Type Inorganic Compounds Resuits(mg/1)
I Environmental Concentrate Comments Arsenic --
bra inc:),,_ d 1 -tc6
Barium --__ Ground water (1) _ Solid (5) Cadmium --Chromium I SE; of s.1+:z. --__ Surface water (2) Liquid (6) Lead --
ss~ 11 ~ --Mercury
V Soil (3) _ Sludge (7) '::>L-Selenium
I --Silver --_ Other (4) _ Other (8)
' --
---I --
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
_ P&T:GC/MS Ar~enic benzene ----. V Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --pc.(3 ----
....t.L <O,J.tJ_pp.~ Chloride chlorobenzene ----Chron:ium chloroform ------
I --__ Copper o-creso!
I --Fluoride m-cresoi ------Iron p-cresol ------Lead crcsol --I --------Manganese --1,4-dichlorobenzene
-Mercury 1,2-dichlorocthane ----
--Nitrate . __ 1,1-dichloroethylene --I Selenium .. . 2,4-dinitrotoluene .. ----Silver heptachlor ----
Radiochemistry Sulfates hexachlorobcnzene ----I .... ,, ___ Zinc hexachlorobut adiene
Parameter ----Results (PCi/1) pH hexachlorocthane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Beta TDS nitrobcnz.cnc ----TOC __ pentachlorophenol ---pyridine ----
I Microbiology --__ tetrachlorocthylene
--__ trichloroethylene
Parameter Results (Col/100111!) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --
AUG 2 8 1997 e/) Reported by
iindanc
I Date Received --
--methoxychlor ,S 'f-'!,J71 k.(., toxaphene --
D:itc Extracted 9-if-97V/' Date Reported --2,4-D
I /JNJIICJ-¥'-"1113,0 973474
2,4,5-TP (Silvcx)
Date An;t!y,c~J1r-971,,p --Lab Number --1)1 IS .11')1 (ltcvi~i.:d 2/91)
N.C. Department of Environment, I , · 11cal1h; &·Natural Resources
. , Sulid W:.!sle M~,'\agement Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
If le Number Alco Ci;; z.._ sss 71 z... Field Sample Number 0·2o 3S()
. . Name of Site S3mo/l :s St'fii'c.... 72-<,;1./c.. Site Location. Sf,:;,Jesvr //e__ I Collected By '::if:'.-ID# ___ Date Collected 9(Zi.c (q7 Time __ (~5_·_?:,_.S __
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds
----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --Barium i31 ~~Ju(\ J_ --__ Ground water (1) _ Solid (5) Cadmium --Chromium I 1),-q,l (\l'.Je.. d,t'-+eA --
__ Surface water (2) _ Liquid (6) Lead --
-J Soil (3) ss-1~,--sL --Mercury
_ Sludge (7) Selenium
I --Silver
_ Other (4) --_ Other (8) . --
--I --Organic Chemistry Inorganic Chemistry --
I Pura meter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Kesults(mg/1)
_ P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmiom chlordane -. Pl/3 ----
...k:_ <O,LOfY"'l Chloride chlorobenzene ----Chromium chloroform ------
I --Copper o-cresol ----
--Fluoride m-crcsol · -----Iron p-cresol ------Lead cresol --I ----
----Manganese --1,4-dichlorobenzene
Mercury 1,2-dichloroethane ----
--Nitrate __ 1,1-dichloroethylene --I Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry· Sulfates hexachlorobenzene ----I ..... ,_., .. _. Zinc hexachlorobutadiene
Pa!"ameter ----Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity methyl ethyl ketone --
I --Gross Beta TDS nitrvbenzene ----TOC __ pentachlorophenol --
----p)Tidine
I Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --
f>O Reported by
lindane
I Dale Received AUG 2 8 1Q97
--
--methoxychlor
. 'W, "/-'()91 14{_,. toxaphene --
D:ilc Exlraclc<l PC8 9-I"-9~ Dale Reported 2,4-0
I --{:J,}f1 9---971!x]) 973475 _ 2,4,5-TP (Silvcx)
Dale Analyzc®-~97Y.P Lab Number --I)! IS Jl'Jl (Revised 2/91)
I , • i:,:.C. D~?J_rtmcnt of Environment,
I lcalth, & Natural Resources
' Solid )Vaslc M<rnagcmcnt Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Hcallh
P.O. Dox 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
.. ,ite Number NCO X z_. s;SS 71 z... Field Sample Number D z_o-3,s (
Name of Site '::ljmo/lS 5.t:f-fi'c_ ffi/1/c.. Site Location Sfq}ey/// //e__ I Collected By l);L,,t ID# ___ Date Collected s/zs(0·7 Time _ _,(_'2,-=-''_-_s __
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Resuits(mg/1)
I Environmental Concentrate Comments Arsenic --
S,ecl;ll'\l'1\+-,
Barium --__ Ground water (1) _ Solid (5) Cadmium --
I 11\_+'
Chromium s-i,etl"-M --__ Surface water (2) _ Liquid (6) Lead --
ck :s,(\-;,_ --Mercury
I V Soil (3) _ Sludge (7) L_.,(X'. s-t· Selenium --Silver
<;;,,. s, -/ l:/ s. D --_ Other (4) _ Other (8) --
I --
--
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) . Organic Compounds Results(mg/1)
_ P&T:GC/MS Arsenic benzene ------L...,-Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --f'(.(3 ----
_kc: <o•IP~ Chloride chlorobenzcnc ----r Chromium chloroform ------
I --__ Copper 6-creso: .. --
--Fluoride m-cresol ----
--Iron __ p-creso1 --
I --Lead cresol ----
----Manganese --1,4-d:chlorobenzcne
Mercury 1,2-dichloroethane ----
--Nitrate __ 1,1-dichloroethylenc
I --Selenium . 2,4-dinitrotoluene ----Silver hcptachlor ----Radiochemistry Sulfates hexachlorobenzene
I ----······-··-Zinc hexachlorobutadiene
Parameter ----Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity __ methyl ethyl ketone
I --Gross Beta TDS nitrot>enzcnc ----TOC __ pentachloropheno! --
--__ pyridine
I Microbiology --__ tetrachloroelhylene
--__ trichlorocthylene
Parameter Results (Col/l00ml) --__ 2,4,5-trichlorophenor
----__ i:,4,6-trichlorophenol
------vinyl chloride
cndrin --
AUG 2 8 1997 13DReported by I
lindane
Date Received
--
--methoxychlor
CM 'I -{3.!i 1 /4:.. loxaphene --D:,tc ExtracteJtfeA' 9-9_-'f_7"J/I' Date Reported --2,4-0
I 6/.Jll-q_ 9-"i76;j 973476 _ 2,4,5-TP (Silvex)
!)ate Anal'['cdl"189-/g-~ Lab Number --1111<,,.' '11!11 /IL • .,;,.,.,, 1/!ll\
, ~.C. DcpJrtmcnt of Environment, I '. I lc.ilth, & Natural Resources
Solid y.'aslc M:inagcmcnt Division
SAMPLE ANALYSIS REQUEST State Laborntory of Public Health
P.O. Box 28047, 306 ~. Wilmington Street
llalcig.h, North Carolina 27611
' .. Site Number Alco O(; z_ sS5 71 Z.. Field Sample Number (0 --Z..o °3,SL
Name of Site Si3mo/l 's Stjz-h'c...-7?vdc.. Site Location Sfq.}ey 1/r l /e.... I Collected By J S ID# ___ Date Collected 't>(Z£/ 11 Time /73'5
I Agency: Hazardous Waste Solid Waste Vs u pc rfun d TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
Sc-l im?1\ .\-
Barium --
Ground water (1) _Solid (5) Cadmium --
I Lu/ l( ietMS' QcJ\ !~
Chromium --__ Surface water (2) _ Liquid (6) Lead --1 Mercury ~<;,,-17 -<;. D --V Soil (3) _ Sludge (7) Selenium
I --Silver --_ Other (4) _ Other (8) --
--I --Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results (mg/I) (mi;/kg) Organic CompGunds Results(mg/1)
P&T:GC/MS Arsenic benzene ------L---Acid:B/N Ext. Bariurp. carbor. tetrnchloride ----MTBE Cadmium chlordane ""t7'" f'.C/3 <"O,ldnz-hl. ----Chloride chlorobenzene ------Chromium chloroform ------
I --Copper o-cresol ----
--Fluoride m-cresol ----Iron __ p-crcsol ----Lead cresol --I ----
--__ Manganese --1,4-dichlorobenzcne
Mercury ' 1,2-dichlorocthane ------
--Nitrate __ 1,1-dichlorocthylcne --I Selenium 2,4-dinitrotol ucne ----Silver heptachlor ----Radiochemistry Sulfates hcxachlorobcnzene ----I ······-·· Zinc hcxaehlorobutadiene
Paramder ----Results (PCi/1) _pH hcxaehlorocthane --__ Gross Alpha __ Conductivity --methyl ethyl ketone
I --Gross Beta TDS nitrobenzcne ----TOC pcntaehlorophenol ----
----pyridine
I Microbiology --__ tctrachloroethylcne
----trichloroethylene
Parameter Results (Col/100ml) __ 2,4,5-triehlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --
f3 [, Reported by
lindane
I Date Received AUG 2 8 1997 --
--mcthoxyehlor
fM-11 q ,g,t/1 tJi --tox3phcnc
D:itc Extracled~ 9-"f-qn(p Dale Reported --2,4-D
I 6 ,<)It 9-9'-9 718 if) 973477 2,4,5-TP (Silvcx)
Dale Analyzed l"'a;> 9-/.:Z-'171/P Lab Number --1)1 lS JJ!J! (H.cvisr.d 2/91)
;:,;.C. Dcp-!rtmcnt of Environment, I ' i lcahh,' &-Natural Resources
. Solid ~aste Ma.iagcmcnt 01V1S1on
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
R..alcig.h, North Carolina 27611
.. ite Nu~ber NC/) Or';; 2..-SS5 71 Z.. Field Sample Number 0'7...0 3,55
Name of Site St3rno//S sr-kc 7q_;1/c__ Sile Location Sfd-er//i //e__
I Collected By /1\ 1-.-ID# ___ Dale Collected £:(rz0(c?1 Time I 1-45
I
I
I
I
I
I
I
Agency: Ha,,ardous Waste Solid Waste Vs u per fund
Sample Type
Environmental Concentrate Comments
__ Ground waler (1) _Solid (5) _ r>p,1 7)1+ 1J:. /
I
__ Surface waler (2) _ Liquid (6) o-e,"
v-Soil (3) _ Sludge (7) S,<:; -/'o -SL
_ Other (4) _ Other (8)
Organic Chemistry
Puramctcr Results(mg/1)
_ P&':':GC/MS
· Acid:E/N Ext.
MTBE
pc_(s
Radiochemistry
Parameter
__ Gross Alpha
Gross Beta
Results (PCi/1)
Inorganic Chemistry
Parameter
Arsenic
Barium
Cadmium
Chloride
Chromium
Copper
Fluoride
Iron
Results(mg/1) (mg/kg)
Lead
Manganese
__ Mercury
Nitrate
Selenium
Silver
Sulfates
Zinc
pH
__ Conductivity
TDS
TOC
1 Microbiology
Parameter Results (Col/lOOml)
I Date Received AUG 2 8 1997 13£) P.eporled by ________ _
fjtA 9-'8-91 ct
D:ite Extractcdtf'M 9-9-97VP Date Reported _______ _
I t;,v,11-9-9-97 6,J) 973478
Date Anilly,cd~9-/-S;'22YP Lab Numbcr ______ ~---
1;11:-.; 111)1 (ltcvi.scd 2j(Jl)
TCLP Compounds
\norganic Compounds
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
Organic Compounds
benzene
carbon lclrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
p-cresol
cresol
1,4-dichlorobcnzcne
1,2-dichloroelhane
Results(mg/:)
Results(mg/1)
------
------
__ 1,1-dichloroelhylenc _____ _
2,4-dinilrotolucnc
hcplachlor _
hexachlorobenzcne
hexachlorobut adicr,e
hcxachloroclhanc
__ methyl ethyl ketone
nitrobenzcnc
__ pcnlachlorophcnol
pyridine
__ lelracn\oroclhylene
__ lrichloroethylene
------
__ 2,4,5-trichlorophenol _____ _
__ 2,4,6-trichlorophcnol ______ _
,inyl chloride
cndrin
lindane
mclhoxychlor
toxaphcnc
2,4-D
__ 2,4,5-TP (Silvcx)
I . f':.C. Dq~;irtmcnt of Environment,
\ lc.illh, & Natural Resources
Solid ~astc Mnnagcmcnt Division
SAMPLE ANALYSIS REQUEST Stale Laboratory of Public Health
P.O. Dox 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611 wile Number_.:M---'--'=c:::.O<-.::.{X;'-"".:;z_.:.._.:;s:_S-=5=--7--'---'1'---Z...-=----Field Sample Number b 'Z.,o 3Sj:
Name of Sile SJ3mo/l s Sy:,kc...-7?uilc.. Site Location Sfqjey VI l /e_
I Collected By /i Z:.. ID# ___ Date Collected 0( '2..(;, ( q 7 Time __ / _':::x'.:) __ s __
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --Barium
be_e1\ r· i-::[+·-z..._ --
__ Ground water (1) _ Solid (5) Cadmium
I --Chromium
I __ Surface water (2) o-G '' --_ Liquid (6) Lead --
V Soil (3) S,s-/lj-SL --Mercury
_ Sludge (7) Selenium
I --Silver
_ Other (4) --Other (8) --
--I --Organic Chemistry . Inorganic Chemistry --
I Parnmeter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
__ P&T:GC/MS Arsenic benzene ----L---Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --ftB ----
.Jc'... <O./QP/'M Cl,loride chlorobenzenc ----r Chromium chloroform ------
I --Copper o-cresol ----
--Fluoride m-cresol --Iron __ p-cresol ----Lead cresol --I ----
----Manganese --1,4-dichlorobcnzene
___ Mercury 1,2-dichloroethane --
--Nitrate __ 1, 1-dichloroethylene --I Selenium 2,4-dinitrotoluenc ----Silver __ heptachlor --
Radiochemistry Sulfates hexachlorobenzene ----I ······-·· Zinc hexachlorobutadienc
Paramelcr ----Results (PCi/1) _pH hexachloroethane
__ Gross Alpha --__ Conductivity __ methyl ethyl ketone
I -· Gross Bela TDS nitrobenzcne ----TOC __ pcntachlorophenol --
--__ pyridine
I Microbiology --__ tetrachloroethylene
--__ trichloroethylcnc
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --
r;f) Reported by
· lindanc
I Date Received AUG 2 8 1997 --methoxychlor --
~"f /B ,1/ 1 ILL toxaphcne
D:i1c Exlraclcd -9-97111' --Date Reported 2,4-0 --
I l3µ,t.J.9-?-'j'7 8£> __ 2,4,5-TP (Silvcx)
D;,tc An;,lyzcd~ Lab Number 97347q --I JI IS Jl1Jl (!lcviscd 2/91)
I .N;C. Di.:p~rtmcnt of Environment,
' 1 lcallh; &· Natural Resources
, Solid Waste Mr,nagcmcnt Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleig.h, North Carolina 27611
wile Number ;(;c.,i) 00 z__ sss 71 z_ Field Sample Number <:2:Z.63.5S
· Name of Site 5J3rno/l S 5t'f-fi 'c., µ;1/c. Site Location SfdeJ Vi/ /e_
I Collected By /\ 'Z.-ID# ___ Date Collected '6( Z 5i 1'7 Time ( e-/ SO
I . Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
Sample Type inorga,,ic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
S[u~/~1·/ Barium ;;;fl_ Solid (5)
--__ Ground water (1) Cadmium --Chromium
I \::>e\0\1c! lutµof\ tl:3 --__ Surface water (2) _ Liquid (6) Lead --J Mercury
S S-c.,, I -Gu .S --
_ Soil (3) V Sludge (7) Selenium
I --Silver --_ Other (4) _ Other (8) --
--I --
Organic Chemistry Inorganic Chemistry --
I Pi~rameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
_ P&T:GC/MS Arsenic benzene ----L-Acid:b/N Ext. BaritJm carbon tetrachloride ----MTBE Cadmium chlordane
/'CB ----v <o,t.()nm Chloride chlorobenzene ----Chromium chloroform ------
I --Copper o-cresol ----
--Fluoride m•crcsol ----Iron p-cresol ------Lead crcsol --I ----
--__ Manganese --1,4-dichlorobenzene
__ Mercury 1,2-dichloroethane ----Nitrate 1, 1-dichloroethylene ------I Selenium 2,4-dinitrotoluene ----Silver heptach\or ----Radiochemistry Sulfates hexachlorobenzene ----
I ······-·· Zinc hexachlorobutadiene
Parameter ----Results (PCi/1) pH hexachloroethane ----__ Cross Alpha __ Conductivity --methyl ethyl ketone
I Gross Beta TDS nitrobcnzcne ------TOC pentachlorophenol ----
----pyridine
I Microbiology ----tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichiorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
cndrin --
Date Recci·,ed AUG 2 8 1997 [3 i\., Reported by
lindane
I --
--methoxychlor
fr.i 9-9-971/P toxaphene
Dale Extracte,lt',,\.4-q_/4'-Q1 ~ --Date Reported --2,4-D
I /J,-.} I'} 9 -I 7 -C/1. 973480 --2,4,5-TP (Silvcx)
D :ii e J\ n a I 'flCd PCB 9-IS-'1?11' Lab Number --1)11.S 31 1)1 (ll.cviscJ 2/9\)
II , .~·.c. Dc_p;i1:1mcnl of Environment, I 1 lcahh, & Natural Resources
SAMPLE ANALYSIS REQUEST State Laborawry of Public Health
P.O. Box 280-17, 3J6 N, Wilmington Street
llBlcigh, Nert],. Carolina 27611 • Solid \Y·ast:: M~nagcmcnt Division
... ilc N umbcr-'-M-"t:..=O-=O(;=-=-=-z_-----'s=---S-=5_7:_1_,__Z.... __ _ Field Sample Number O'?_o?,S(,
Site Location SfdeJ /// / /e_ · Name of Si1c_S;_z13"'l' '-'-m-"o"'//'-'...=.5'--~Y'f=:..:-f,_:_'..::c...:::__,7ac="-/!-"/,'--c_"---
.· • ·· Collected By /)/,IJ ID# ___ Date Collected 0/z1.p ( '1] Time~Q~6~/ £=-cC:...) __
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
s(ucB e /s() l I
Barium --
__ Ground water (1) ~Solid (5) Cadmium --Chromium I pelow / ,•[JXA -#-c --
__ Surface water (2) _ Liquid (6) <.J Lead --
ss-27.-(,,US
__ Mercury
·_Soil (3) V Sludge (7) Selenium
I --Silver --_ Other (4) _ Other (8) --
--I --
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
_ P&T:GC/MS Arsenic benz:ne ----C---Aeid:B/N Ext. Barium carbon tetreehloride ----
MTBE Cadmium chlordane --Pee; ----
--1.c <0./0 /Jo/"'--Chloride chlorobenzenc ----Chromium chloroform ------
D --__ Copper· o-cresol --
--Fluoride m-crcsol ----Iron __ p-cresol ----Lead crcsol --I ----
--__ Manganese --1,4-dichlorobenzene
__ Mercury . 1,2-dichloroethane ----
--Nitrate · __ 1,1-dichloroethylene --I Selenium 2,4-dinitrotoluene ----
Silver heptachlor ----
Radiochemistry Sulfates hexachlorobenzene ----I ······-··-Zinc hexachlorob11tacliene
Parameter ----Results (l'Ci/1) pH hexachloroethane ----__ Gross Alpha --Conductivity __ methyl ethyl ketone
I --Gross Bela TDS ni~robenz.cnc ----
TOC __ pcntachlorophenol --
----pyridine
I Microbiology ----tetrachloroethylene
----trichloroethylene
Paramctl'r Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----__ ,inyl chloride
cndrin --
I AUG 2 8 tl97 eiiD Reported by
lindanc
Date Received --methoxychlor
,f't'J3 q-i:J-?71/P -· __ toxaphene
D:,tc Exlraclcu t,M:: %-1'91u---: Dale Reporleu 2,4-0 --131,1,q -(7-CJ1&.J) 973481 __ 2,4,5-TP (Si!vex)
Dale Analy,edPf!89-/9-?7V/! ___ Lab Number --I
!) I IS :i I 1J! ( l{cviscd 2/91)
I , N.C. Dcp:H:mcnt of Environment,
I lc.ilth, & Natural Resources
' Solid \l..'iisle Ma'nagc.mcnt Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
llaleigh, North Carolina 27611
m.tle Number----'M-"'c"'o'--"'00---"'---.::..z___sc__s_s_...c.7_</,__2-. ___ Field Sample Number b '2.,03,S 2
Name of Site SJ3rno/l S Stjz·kc ?a,;1/c.. Site Location Sfde,s 1/i / /e... I Collected By s~ JD# ___ Dale Collected Q/Z(p ( 17 Tim~ L a{--z..
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --Barium
~lid (5) s (.1 d lj e... pt/c. --__ Ground water (1) Cadmium
I --J Chromium I C, /' -18/1 --
__ Surface water (2) _ Liquid (6) I Lead --
ss--z..:~-w.s __ Mercury
_ Soil (3) VSludge (7) Selenium
I --Silver --
_ Other (4) _ Other (8) --
.
I --
--
Organic Chemistry Inorganic Chemistry --
I Purnmcter Results(mg/1) Parameter Results (mg/l)(rug/kg) Organic Compounds Results(mg/1)
_ P&T:GC/MS Arsenic benzene ----
L.--Acid:B/N Ext. Barium carbon tetrachloride ----
MTBE Cadmium chlordane --Fe/.? ----
....iL <o,{.O_R,R/1'\ Chloride chlorobenzene ----Chromium chloroform ------
D --__ Copper o-cresol --
--Fluoride m-cresol ----
--Iron p-cresol ----
I --Lead crcsol ----
--__ Manganese 1, 4-d icr. I orobenzene --
--__ Mercury --1,2-dichloroethane
Nitrate 1, 1-dichloroethylene --I ----Selenium 2,4-dir,it rotoluene ----
Silver heplachlor ----
Radiochemistry Sulfates hexachlorobenzene
I ----..... ·-··----· Zinc hcxachlorobutadiene
Parameter ----Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Bela TDS nitrobcnzcnc ----TOC __ pcntachlorophenol --
----pyridine
I Microbiology --. --letrachloroethylene
----trichlcroethylene
Parameter Results (Col/lO0ml) 2, 4 ,5-tri ch lorophenol ----
----__ 2,4,6-trichlorophenol
--__ viny} chloride
endrin --
. 13D I lindane --Dale Received AUG 2 8 1997 Reported by mclhoxychlor
l'l!/3 9-9-:-971/P --. __ lor.aphene
Date Exlracteu(½.4--q -q-q11??: Date Reported 2,4-D
I --/{jf'"C/-1 7 -~7 8iJJ 973482 -· 2,4,5-TP (Silvcx)
Dale Analyzed ?46:9_zyp Lah Number
111 I<..; < 1 rJl ( I) ,-.,;,.,.,I "l /(JI\ --
.~.C. Ocp,artnu:nt of Environment,
I ' l lc:ilth', & Natural Resources
. Solid ".-'.astc M:1nagcmcnl Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
C' .-, , ~·2 c;;c:o' Field Sample Number u ~~.::,~ --=----~---------•• ile Number /\Jc,/) D(; 2--SSS 7'7 z_
. Name of Site Si3rno// S Stpkc 7?{;1 /c.. Site Location Sfqfcy Vr '( /e_
I Collected By /'\ 1,. ID# ___ Date Collected 0r-(_-z._&_(_a_, _l ___ T_i_m_e::::::::_l_,_(...cf::_'8"-_-:_-:_-:::_:_,
I
I
I
I
I
I
I
I
Agency: Hazardous Waste Solid Waste Vsuperfund
Sample Type
Environmental Concentrate Comments
__ Ground water (1) ~olid(5)
I
__ Surface water (2) _ Liquid (6) ·z_ F+
_ Soil (3) ~Sludge (7)
_ Other (4) _ Other (8)
Organic Chemistry Inorganic Chemistry
Purnmeter Results(mg/1) Parameter Results(mg/1) (mg/kg)
_ P&T:GC/MS v· Acid:B/N Ext.
MTBE pc.(3
Arsenic
Barium
Cadmium
Chloride
Chromium
Copper
Fluoride
Iron
Lead
Manganese
1--------l
Radiochemistry
__ Mercury
Nitrate
Selenium
Silver
Sulfates
Zinc I Parameter
__ Gross Alpha· -------
Results (l'Ci/1)
Gross Beta
Microbiology
Parameter Results (Col/lOOml)
pH
Conductivity
TDS
TOC
. BD
I Date Received AUG ~8 :1992 Reported by ~<!8 9-9-971/~ -------
D:ilc Extracted f;.11A-q ,.q 41 /(J?-D:ile Reported _______ _
I 6JJfr9-t7-9J/llil 973
Dale Analyzed Pea 9-/6--970" Lab Number 483
1)1 JS )l'JI (IZcvi.~cci 2/91)
TCLP Compounds
Inorganic Compounds
Arsenic
--
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chiordane
chlorobenzene
chloroform
o-crcsol
m-crcsol
p-cresol
crcsol
1,4-dichlorobenzene
--1,2-dichloroethane
Results(mg/1)
Results(mg/1)
------
------
__ 1,1-dichloroethylene _____ _
2,4-dinitrotoluene
heplachlor
hcxachlorobenzene
hexachlorobu ladiene
hcxachloroelhane
__ methyl ethyl ketone
nitrobcnzcne
__ penlachlorophenol
pyridine
__ telrachloroethylene
trichloroelhylene
__ 2,4,5-trichlorophenoi
__ 2,4,6-lrichlorophenol
vinyl chloride
endrin
l:ndane
melhoxychlor
loxaphcne
2,4-D
__ 2,4,5-TP (Silvcx)
------
I , :-' .. C. Dcpa~tnicnt of Environment,
1 lcallh, & Natural Resources
· Solid \1/itstc Mahagcmcnt Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wi:mington Street
R..aleigh, North Carolina 27611
.. le Number NCO Ct;; z... . sss 71 z_ Field Sample Number ___ o_·z__o_3s_+2---~---
. C' _r I V/Jf, --r:,. I s,J..-I --·( I · Name of Site Yjrl10/IS -=r 'c:... J0,/l/C.. Site Loeation _ __,_.,·:..:,,':'.':-TT:'.l'-'-'-""'-~'-'-1_,_,_/i.,,e_==------------1 Collected By h 'L.. ID# ___ Date Collccted _ __c0c.-,_(--i_(p_,_(_,_t/_1--' __ Time _ __c/_' o----=:s:.,rc___
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concfntrate Comments Arsenic --
~olid(5) _ S( ucfg.e
1
p1le Barium --
__ Ground water (1) Cadmium --Chromium I be.1~ 3 feec-/---
__ Surface water (2) _ Liquid (6) Lead --
'SS---z,5 -LUS
__ Mercury
I _ Soil (3) V Sludge (7) Selenium --Silver
_ Other (4)
--
_ Other (8) ----I --
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
_ P&T:GC/MS Arsenic benzene ----
..JL Acid:B/N Ext. Barium carbon tetrachloride ----
MTBE Cadmium chlordane --IZB --
_IL: <O•lP~ Chloride chlorobenzenc ----Chromium chloroform ------
I --_-_Copper o-crcsol --
--Fluoride m-crcsol ----
Iron __ p-crcsol ----Lead cresol
I ------
--__ Manganese 1,4-dichlorobcnzcne --
--__ Mercury __ 1,2-dichloroethane
--Nitrate __ 1,1-dichlorocthylenc
I --Selenium 2, 4-dinitrotol ucne ----Silver __ hcptachlor --Radiochemistry Sulfates hexachlorobenzenc ----I ······-·· Zinc hexachlorobutadiene
Parumcter ----Results (PCi/1) _pH hexachloroethanc --__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Beta TDS ni~robenzcne ----TOC __ pentachlorophenol --
--__ pyridine
I Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/!OOml) __ 2,4,5-trichlorophenol --
----__ 2,4,G-trichlorophenol
----__ vinyl chloride
end:-in --
I Date Recciv~ Reported by
lir.danc --__ methoxychlor
9-9-'177/P . toxaphcnc --
Date Extractcc~~;::~ Date Reported 2,4-D
I --
973484 --2,4,5-TP (Silvex)
Date Analy-;,ed -;_ ~ Lab Number --
I \ I : <...: 1. 1 I)) I \I,...;,.,,,! "J /t)l \
I . ·t>-:.C. Di;p.i.nmcnl o( Environment,
] lcallh, & Natural Resources
' So!id Waste Miinagcmcnt Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Field Sample Number _____ O_'"Z..._0_-_?:,_(,_6 _____ _ .. ile Number-'-M-'--'r,""i)"'-=-~---=-=Z...=--· -=-s_S-=5__;7_C/,__L __ _
Name of Site S,;3mo// s Yfn'c... 7alllc.. Site Location Sfqfesvr l le...
Collected By _____ f,_'l'--l=-·----ID# ___ Date Collected Cb(z& (q7 I Time_/,__0_,5~f __ _
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
,S( 0c( c1.e. ;;1 /z_ Barium
~Solid (5)
--
__ Groundwater (1) Cadmium _:,; I --
I Chromium /)_Je_/,' [c}p__ l ::, t-f. --
__ Surface water (2) _ Liquid (6) Lead
I < --
SS-/"2-S -ws: --Mercury
I _Soil (3) V Sludge (7) Selenium --Silver --
_ Other (4) _ Other (8) --
I --
--
Organic Chemistry Inorganic Chemistry --
I Purnmcter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
_P&T:GC/MS Arsenic benzene ----
L--Acid:B/N Ext. Barium carbon tetrachloride ----
MTBE Cadmium chlordane --Pct, ----v <0,/0./'f2t!:!. Chloride chlorobenzeue ------Chromium chloroform ------
I __ Copper --o-crcsol
--Fluoride m-cresol ----Iron __ p-crcsol ----
I --Lead cresol ----
--__ Manganese 1,4-dichlorobenzcne --
--__ Mercury --1,2-dichlorocthane
--Nitrate -__ . 1,1-dichloroethylenc
I --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene
I ----······-·· Zinc hexachlorobutadiene
Parameter ----
Results (PCi/1) _pH hexachloroelhane --
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I Gross Bela TDS nitrobenz.cnc ------TOC __ pentachlorophenol --
--__ pyridine
I Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/JOOml) __ 2,4,5-trichlorophenol --__ 2,4,6-trichlorophenol ----
----__ vinyl chloride
cndrin --
I AUG 2 8 1997 J, () Reported by
lindanc
Date Received
--__ methoxychlor
R!l8 q-9-97V7' __ toxaphene
I D:ilc Extracicd~A-q _/l,</1 ~ Dale Reported --2,4-D
~;'I Cflij'.q 1 ,() 973485 __ 2,4,5-TP (Silvcx)
Dale i\n«lyzcd~-/9-2ZJ.'P Lah Number --I\ I I<: '.l 1111 /I)~.,:,,,,,! '.l /0 I 1
I . :':C. Depurtment of Environment,
I lea Ith, &" Natural Resources
· Solid V{'aslc Mi:nagcment Division
SAMPLE ANALYSIS REQUEST State Laboratory o( Public Health
P.O. Box 28047, 306 N. Wilmington Street
Ral.:igh, North Carolina 27611
· If ite Number....'.Ni_::_ocL-:;.OL...::D(;:.=,:::2.-c_____:S:::::.....:S:..:5=-...:7--'1'-Z...-=---Field Sample Number __ .1...Q"-Z0=--_3_(,-'--'--(--'---------
, c r r Vo.1' --r:,, f . . SJ. I. •( I Name of Site Yjfl1o/lS --=-Fn c... Jq/lfC.. Sile Locatwn ~1?<.Te:fVI fe.....
I Collected By h -z.__ ID# ___ Date Collected £(z_r; (,17 Time / ( f1-
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
Sv,F,,,__ce I Barium
.S01 --
__ Ground water (1) _·_ Solid (5) Cadmium --
I a.ct:().c-e!\+ -f';,) Chromium --
__ Surface water (2) _ Liquid (6) Lead --
V Soil (3) SltY'Mje, 77t ~~-~ (-ti,) __ Mercury
I _· _ Sludge (7) Selenium --v Silver S S-7.&;-S.C --
_ Other (4) _ Other (8) --
--I --
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results (mg/!)(mg/kg) Organic Compounds Results(mg/1)
_ P&T:GC/MS Arsenic benzene ----v-Acid:B/N Ext. Barium carbon tetrachloride ----
MTBE Cadmium chlordane --fL/3 ----(..,-< tJ, lo -fllD" Chloride chlorobenzene ------Chromium chloroform ------
I --__ Copper o•cresol --
--Fluoride m-crcsol ----
--Iron __ p-cresol --Lead cresol
I ------
--__ Manganese --1,4-dichlorobenzene
__ Mercury 1,2~dichlorocthane ----
--Nitrate __ 1,1-dichloroelhylene
I --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----I ······-··-· Zinc hexachlorobutadiene
Parameter ----
Results (PCi/1) pH hexachloroelhane ----
__ Gross Alpha --Conductivity __ methyl ethyl ketone
I Gross Beta TDS nitrobenzcnc ------
TOC __ pentachlorophenol --
----pyridine
I Microbiology ----tetrachloroethylene
--__ lrichloroelhylene
Parameter Results (Col/1001111) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --
I Date Received AUG 2 8 1997 /?IO Reported by
lindane --melhoxychlor
!PCB 9-'1-971/P --__ toxaphene
D"te Exlractecl,5,1.A--';1-// ..c;1 {_Uc--Dale Reported --2,4-0
I [J,v,4 9 -,f?-9 J 8',/) 973486 __ 2,4,5-TP (Silvcx)
Date Analy,cdlJ:Jl.!l::~97]/P Lab Number --
1)11'-: 111/1 (HrviH·d J/()1'\
I . 'l':.c. Dsp•ipmcnt of Environment,
1 !c:illh, & Natural Resources
· Solid Waste Ma'nagcmcnt Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. llox 28047, 306 N. Wilmington Street
R.eleigh, North Carolina 27611
.. ilc Number-'M--"c:...i)<-.-::Qjc.=..::2-_ _cs_S_5 _ _;_7~1:...-2-___ Field Sample Number 07-0 °3,b -z_
Name of Site SJ3rno// S St'f-li 'c:... 7?,;1,/c.. Site Location Sfq..fey //1 '( /e_
I Collected By SI::-ID# ___ Date Collected 'Wz<r ( C?1 Time { If(:,
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
Sur¼ce SD( I Barium --__ Ground water (1) _ Solid (5) Cadmium --
I Chromium ,, + --t-0 --
__ Surface water (2) _ Liquid (6) O 1.Jerc e,--Lead --
V Soil (3) ~-1-lf'vf§: -rtl,K,,b "'ik:f: __ Mercury
I _ Sludge (7) Selenium --Silver
-SS-?'1 -SL---
_ Other (4) _ Other (8) --
I --
--
Organic Chemistry Inorganic Chemistry --
I Parameter Rcsults(mg/1) Parameter Results (mg/l)(mg/kg) Organic Compounds Results(mg/1)
_ P&T:GC/MS Arsenic benzene ----Acid:B/N Ext Barium carbon tetrachloride ----
MTBE Cadmium chlordane --PC/$ ----v <O, IO /'I!-'"-Chloride chlorobenzene ----Chromium chloroform ------
I --__ Copper o-cresol --
--Fluoride m-cresol ----
--Iron p-cresol ----
I --Lead cresol ----
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-diehloroethane
Nitrate 1, 1-dichloroethylenc --I ----Selenium 2,4-dinitrotoluene
. ----
Silver heptachlor ----
Radiochemistry Sulfates hexachlorobenzene
I ----······-··-Zinc hexachlorobutadiene
Parameter
----Results (PCi/1) pH hexachlorocthane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
I --Gross Beta TDS nitrobcnzene ----,TOC __ pentachlorophenol --
--__ pyridine
I Microbiology ----tetrachloroethylene
----trichloroethylene
Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol.
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --
I pj) !indanc
Date Received AUG 2 !! 1997
--
Reported by __ methoxychlor
I'~ q-9 -97VP __ toxaphcne
I
Dale Exlracledfal,4 '1 'lff1 ~ Date Reported --2,4-D
tJ~,1r 9-t Y-9 7 8Q 973487 --2,4,5-Tf' (Silvex)
Dale Anai'f1.edectl9_-~977/P Lab Number
1'1!<..' 11111 /11,. .. :,,, .. 11/'!1\ >
--
I, : :"'-C. D,CJ~.lrtment of Environment,
l lca\th, & Natural Resources
· Solid y;astc Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Field Sample Number ___ _:0=--Z...-=-o_j,b=-c:c5:c_ ______ _ .. ite Number---'-M-'--c=o'----or;;=-><-=z....=-----=s-S----'5=----'7_'1,___Z... __ _
· Name of Site_S,.....zc,j,q.m"-'-'o'-'-/1~..S:__=Yf=:....1).:...'.:::c...::..__,ffi-=.,_;1'-'/<_c..:___ Site Location. _ _:Sc-1.:i.::.¼2.0""--'~'-'-1 1.../1.:/ e_=---------1 Collected By ';> k.-ID# ____ Date Collected __ 9:/-'----z._b--'{'--q_7 ____ Time __ (_-Z.._o_S __ _
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
/JO(,u!\ ~\ ("'-L~t't-,J--d._:,_ Barium --__ Ground water (1) Solid (5) Cadmium --Chromium
I Yw0:f 'Tl{,Jc.& --__ Surface water (2) _ Liquid (6) Lead --
1x,ptl, ~-~ 1(2. ft--__ Mercury
VSoil (3) _ Sludge (7) Selenium
I --Silver
SS. -Z 'c.1-SL --
_ Other (4) _ Other (8) --
--I --
Organic Chemistry Inorganic Chemistry --
I Parumeter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
_ l'&T:GC/MS Arsenic benzene ----(,....Acid:B/N Ext. Barium carbon tetrachloride ----
MTBE Cadmium chlordane
---c Pc.8 ----<O,/Opj?m.. Chloride chlorobenzene ------r Chromium chloroform ------
I --Copper o-crcsol ----
--Fluoride m-cresol ----Iron p-cresol ------Lead cresol
I ------
--__ Manganese --1,4-dichlorobenzcne
__ Mercury 1,2-dichloroethane ----Nitrate 1, 1-dichloroethylene ------I Selenium 2,4-dinil rotoluene --Silver __ heplachlor --Radiochemistry Sulfates hexachlorobenzene ----I ······-·· Zinc hcxachlorobuladicnc
Parameter ----
Results (PCi/1) pH hexachlorocthane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
I --C,ross Beta TDS nitrobenzcnc ----
--TOC __ pentachlorophcnol
----pyridine
I Microbiology --__ tctrachloroethylcne
----trichloroethylcne
Parameter Results (Col/1001111) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --
I AUG 2 8 1997 (3 0 Reported by .
lindane
Dale Received --__ methoxychlor
l:JIA-'f-11 ~ Cf1 U..,... toxaphcne
D:ilc ExlraclcdJi:2J 'l-/.,i-9'7~ --Date Reported 2,4-D
I tJ,,14 9-/Y>IJl.3 973488 _ 2,4,5-TP (Silvcx)
Dale /,naly1cdf'4_3~ Lab Number --1)11<-: 1,Jl)I {llr,,ic,,,i 'J/!Jl)
I. S.C. D~p..i_rtment of Environment,
I lcal!h, & Natural Resources
· Solid Waste M<inagcmcnt Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
..,ite Number Neb er;; 2.-sS5 717_ Field Sample Number o·z_030f
Name of Site SJ3rno/l S St:(-h'c__ ffi/l/c_ Site Location Sfq/-esn //e_ I Collected By sl-ID# ___ Date Collected gjzs,/ "'(7 Time __ /_··~_7 __ _
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
Sample Type InofJlanic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
o . d so, I Barium --
__ Ground water (1) _ Solid (5) /::ac,~C\ . Cadmium --Chromium I -z {/ -?,,, ( bct-M --
__ Surface water (2) _ Liquid (6) Lead --
SS--zq-sL --Mercury
. V Soil (3) _ Sludge (7) Selenium
I --Silver --_ Other (4) _ Other (8) --
--I --
Organic Chemistry Inorganic Chemistry --
·1 Pam meter Results(mg/1) Parameter Results (mg/I) (mg/kg) 0fJlanlc Compounds Results(mg/1)
_ P&T:GC/MS Arsenic benzene ----
_L.Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane --PW ----
~ < 0 . / 0 .Rf!!!J. Chloride chlorobenzene ----Chromium chloroform ------
I --Copper o-crcsol ----
--Fluoride m-crcsol ----Iron p-crcsol ------
I --Lead cresol ----
----Manganese --1,4-dichlorobenzene
_._ Mercury 1,2-dichloroethane --
--Nitrate __ 1,1'.dichloroethylene
I --Selenium 2,4-dinitrotoluene ----
Silver · __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----I .. , ... ____ Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroelhane ----
__ Gross Alpha __ Conductivity · __ methyl ethyl ketone
I --Gross Beta TDS nitrobenzcnc ----TOC __ penlachlorophenol --
----pyridine
I Microbiology ----tet.rachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --
I eJf). Reported by
lindane
Dale Received AUG 2 8 1997 --
--methoxychlor
lf.-/J, qr// "/ 'J t::,.£--toxarhcnc
D:ilc Exlracle<lPCB <J.-L,;z.-<r,J/P --Date Reported --2,4~D
I &JJA 9 -I .r' '17134) 973489 __ 2,4,5-TP (Silvcx)
Date Analy1.cdf(IJ9-l7·971/,0 Lab Number ------I )I I'-: 11 1)1 (lfrvi-:rd 1/()\]
'
I
I. i·;.c. D~p~r.tmcnt of Environment,
I lcallh, & Natural Resources
· Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
.. le Number Ne)) Dr;; Z... sss 71 z... Field Sample Number O 20·~~5
Name of Site S13rno/l s 'Sqzkc 72utlc..
I Collected By st-ID#
Site Location Sfqjesvi //e__.
Dale Collected 0/ U / 11 Time (3-.s7 '
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
/3,:i c ½}swt't:;/ Sn r '( Barium --
__ Ground water (1) _Solid (5) Cadmium --Chromium I '> (h--1--1 der ff----
__ Surface. water (2) _ Liquid (6) Lead --
,SS -:::0 ~ SL,
__ Mercury
V Soil (3) _ Sludge (7) Selenium
I --Silver
_ Other (4) --_ Other (8) --
--I --
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
_P&T:GC/MS Arsenic benzene ----
L,.Acid:B/N Ext. Barium carbon tetrachloride ----
MTBE Cadmium chlordane --f'C/3 --
__k <o./0#-"" Chloride chlorobenzene ----Chromium chloroform ------
I --__ Copper o-cresol --
--Fluoride m-crcsol ----
--Iron __ p-cresol --Lead cresol
I ------
--__ Manganese 1, 4--dich lo robenzene --
--__ Mercury --1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylene
I --Selenium 2,4-dinitrotoluene ----Silver __ heplachlor --Radiochemistry Sulfates hexachlorobenzene ----I ... ,.,_,,_ Zinc hexachlorobutadiene
Parameter ----
Results (PCi/1) _pH hexachloroethane --
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Bela TDS nitrobenzene ----TOC __ pentachlorophenol --
--__ pyridine
I Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophcnol
--__ vinyl chloride
endrin --
I Dale Received · AUG 2 8 ~6)Reportcd by
lindanc --__ methoxychlor
. {!,1'//---4 ~ 1,q1 · __ toxaphcnc
D,lle Extracted&' 7-J.:i.-171/P Dale Reported 2,4-D
I tJrJ,49--t fl-97 8i.J) --
973490 __ 2,4,5-TP (Silvcx)
Dale Analyzed Pe.LI 'l_-17-971!'.P Lab Number --l)!!S 11 1)! i!tcvist:d 2/9\\
I , .N.C. D7par.tmcnl of Environment,
I lc.illh, & Natural Resources
. Solid Waste Ma'nagcmcnt Division
SAMPLE ANALYSIS REQUEST
sSS 712-Field Sample Number
State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
tYZ-6?/4C::, •• le Number Alco 00 z.._
Name of Sile ~r I '(Jrno/lS Sfkc:..-74;t/c.. Sile Location Sfdesv1 '//e_
I Collected By Ste ID# Dale Collected 0o{zS,[cfl Time /4/o
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
~J:"&~ ~\J 1 '· I
Barium --
__ Ground water (1) _ Solid (5) Cadmium --
I Chromium
I 'L ft . deft:'. --
__ Surface water (2) _ Liquid (6) Lead --
\/soil (3) SS -·3, I ~ S. L
__ Mercury
I _ Sludge (7) Selenium --Silver
_ Other (4) --_ Other (8) --
I --
--
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
_P&T:GC/MS Arsenic benzene ----JeAcid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------V (C/3 <O,IDfPn1. Chloride chlorobenzcne ------Chromium chloroform ------
I --__ Copper o-cresol --
--Fluoride m-cresol ----
--Iron p•cresol ----
I --Lead cresol ----
--. __ Manganese 1,4-dichlorobenzene --
--__ Mercury --1,2-dichloroethane
Nitrate 1, 1-dichloroethylene --I ----Selenium 2,4-dinitrotoluene ----Silver hcptachlor ----
Radiochemistry Sulfates hexachlorobenzene.
I ----
.. ···-··-Zinc hexachlorobutadiene
Paqunclcr ----Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Beta TDS nitrobcnzcnc ----TOC pcntachlorophenol ----
----pyridine
I Microbiology ----tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophenol
---__ vinyl chloride
en<lrin --
I AUG 2 8 1997 ~ Reported by
lindane
Date Received
--mcthoxychlor --
/!/'-4 "I-ff-? 714:,, __ toxaphene
Date Extracted f'f'.B <f'-J,?.-1/71/',0 Dale Reported 2,4-D
I ,Jt-lA-q 19-91 /3;{)
--
973491 __ 2,4,5-TP (Silvex)
Dale A naly-1.ed PCB 9-L7-97VP Lab Number ---I\ I J<.: 11 Cl 1 ( 11 ,.,.;,.,,d ; /01 \
I , '; N.C. 1/cp~rtmcnt of Environment,
\ lcalth, & Natural Resources
' Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 2&047, 306 N. Wilmington StreC:"t
Raleigh, North Carolina 27611
..,ite Number Neb Q;; z_ sS.5 71 z__ Field Sample Number O 7 __ e, '?>0 7
Cj I Stp-h 'c_ Tt).;'t/c._ Site Location Sf des VI '( /e__
I
I
I
I
I
I
I
I
'Name of Site ~rno/lS
Collected By JS JD# Date Collected ca{zi' ( Cf1 Time / 'o'2S:.
Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds
Sample Type
Environmental Concentrate Comments
_ Ground water (1) _ Solid (5) ":.±' di'rvi e{\+
_ Surface water (2) _ Liquid (6) /?,e/0.,0 M•Yl foe.r[fA
V Soil (3) _ Sludge (7) --+r=--=--.,_,C::,_f: ______ _
_ Other ( 4) _ Other (8) S,S---[ / b -S (j
Organic Chemistry Inorganic Chemistry
Inorganic Compounds
Arsenic
Barium
Cadmium
Chromium
Lead
__ Mercury
Selenium
Silver
Parameter Results(mg/1) Parameter
Arsenic
Results(mg/l)(mg/kg) . Organic Compounds
benzene
Results(mg/1)
Results(mg/1) _ P&T:GC/MS
L/Acid:B/N Ext.
MTBE
· Barium
Cadmium
Chloride
Chromium
_______ . carbon tetrachloride -I --chlordane -------'-,-·· PC/3 <0,/01'j'nt . ,
__ Copper
Fluoride
Iron
Lead
chlorobenzene
chloroform
o-cresol
m-crcsol
__ p-cresol
cresol
1,4-dichlorobenzene
1,2-dichloroethane -------
I t---------l
__ Manganese
__ Mercury
Nitrate
Selenium
Silver
Sulfates
f
--1,1-dichloroethylene
2,4-d initrotol uene
__ heplachlor
hexachlorobenzene
__ hexach\orobutadiene
-------
I
I
Radiochemistry
Parameter
Zinc
Results (PCi/1) _ pH
__ Gross Alpha
Gross Beta -------
__ Conductivity
TDS ---~--
TOC
I Microbiology , ___ ____j I
I
I
Parameter Results (Col/lOOml)
Dale Received AUG 2 8 1997 /c3~eporlcd by f!/lfr 9 ~r$· q'1IUC ---------
0:ilc Exlraclc~,4.q9;~J'fJf/f Dale Reported _______ _
Dale An«l·p.cdeCB9-/7--97Vp Lah Number 973492 ll I' 11( flfrvi~1· 11 q1\
hexachloroethane ------,
__ methyl ethyl ketone
nitrobenzene
__ pentachlorophenol
__ pyridine
__ tetrachloroethylene
__ triehloroethylene
__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol
--vinyl chloride
endrin
lindane
__ melhoxychlor
__ toxaphene
2,4-0
_ 2,4,5-TP (Si/vex)
----
---
g .:~.C. Qc~:i.rtmcnt of Environment,
1 lcallh, & Natural Resources
, Solid \:fasle Mdnagement Division
SA_!'ilPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box: 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Field Sample Number ___ C>_Z_Ci____cZ_.C;_Q=---------.. ile Number /VC.L) {X; 2.-SS5 71 Z...
Name of Site Stjmo/1 S 5Lt'·kc 72),;i/c._ Site Local ion SfcJ-e.s //1 / /e_
I Collected By ])uJ ID# ___ Date Collected <!r5(Z.i.o / t?;
I Agency: Hazardous Waste Solid Waste VSuperfund
Sample Type
I Environmental Concentrate Comments
__ Ground water (1) _ Solid (5) S/ uc!ge St '"f /e_
I __ Surface water (2) _ Liquid (6) ~00\\. #-'S
_ Soil (3) V Sludge (7) \)¼'~ [o-ll tE'ef
I Other ( 4) _ Other (8) S,S-'YS--\iu s
I Organic Chemistry Inorganic Chemistry
fn Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg)
U _ P&T:GC/MS
\.....-Acid:B/N Ext.
Arsenic
Barium
I
I
MTBE
v pC./5
Cadmium
Chloride
Chromium
_. _.Copper
Fluoride
Iron
Lead
__ Manganese
__ Mercury
li---------l
Nitrate
Selenium
Silver
Sulfates
Zinc
Radiochemistry
I Parameter Results (PCi/1) pH
__ Gross Alpha -------Gross Beta
Microbiology
Parameter Results (Col/lO0ml)
__ Conductivity
TDS
TOC
I Date Received AUG 2 8 1197 rai9 Reported by _______ ~_
Mil-c;-1 t-<t 1 u... .
Date ExlraclcJ ;oea 9--12-VVP Dale Reported
I /,$;.J,49-/'1-97 .a.{) ------
. Dale Analy1.cd l'CB 9 17--97'Vr"__ Lab Number 973493
l)IIS :WJI (!tcviscd 2/!Jl) ------~---
Time D-?(u ~----------------
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
--Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-crcsol
__ p-cresol
cresol
1,4-dichlorobenzene
1,2-dich loroethane
Results(mg/1)
Results(mg/1)
------
------
1,1-dichloroethylene _____ _
2,4-dinitrotoluene
heptachlor
hexachlorobenzene
hexachlorobutadiene
hexachloroethane
methyl ethyl ketone
nitrobenzene
__ pentachlorophenol
pyridine
tetrachloroethylene
trichloroethylene
2,4,5-trichlorophenol
__ 2,4,6-trichJorophenol
vinyl chloride
endrin
lindane
mcthoxychlor
toxaphcne
2,4-D
2,4,5-TP (Silvcx)
------
I STATE LABORATORY OF PUBLIC HEALTH
P.O. BOX 28047 -306 N. WILHINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEHICAL ANALYSIS
/NEUTRAL AND ACID LAB NO :;;;~ Lf'/3V7/. '-f7-?(/ ZJ '173'17~ '17 Y.N
EXTRACT ABLES FIELD # o?6.-:?IJ• ;;)03u11r .::Jn~'/ll .;10:.. :Jt.,:;
COIIPOUND TYPE ( ~) ( :,, \ ( =t) ( -~) ( '3)
--;;,,.,;( "n / kn .. ,.,-i':',n/ka .. ~n/kn ~, ✓ /ka -,1?11'Y., o/ko UNITS
N nitrosodirrethvlamine to/ ::,,iA I -., IA I A -
b. (2-chloroethvllether -
f hlor~henol
E nol
1 3-<lichlorobenzene
1 -<lichlorobenzene
) -dichlorobenzene
bis (2-ch loroi =r~vl )ether
h achloroethane
N itroso-<li -n-nroovlami ne
nitrobenzene I nhorone
itr~henol
2 -<lirrethvlohenol
bis(Z-chloroethoxvlrrethane
-<l i ch l orooheno l
I 4 trichlorobenzene
naphthalene
Bfchlorobutadiene
h l oro-<n-creso l
~lorocvcl=ntadiene
tri ch lorooheno 1
hloron>nhthalene
a~n•0 hthvl ene
dirrethvl ohthalate
1-<linitrotoluene
naohthene
2 4-<linitr~henol so, '050
1-<linitrotoluene 10, ?'10
itr~henol -01 .,,_co
fluorene 10/:230
! hlor~henvlohenvlether
( thvl ohthalate 'I
'•· -dinitro--o-cresol so ~r--o
di henvlami ne 10,330
nzene ..
r~henvlohenvlether
hexachlorobenzene ~
tachloroohenol so/N,:ro
nanthrene I/I ✓?--~0
anthracene
utvl ohthalate , . I I J
oranthene ,, ' ' ' ·, \
ml>L
'
Estimated value. l-{,.o/.S0/1,..
Actual value is known to be less than value given.
Actual value is known to be greater than value given .
. ,U -Haterial was analyzed for but not detected. The nurber is the Hininun Detection Limit. m])L ---
)
-Not analyzed.
-Tentative identification.
-On NRDC List of Priority Pollutants.
I
(j)
<?73'1 /',
...:Jo3.S-C>
(-3)
, ~"uO"tko )
' ,t -
/
\
I ..
I
I
I
I
BASE/NEUTRAL AND ACID
EXTRACT ABLES
COIIPOJND
nvrene
benzidine
butvl benzvl ohthalate
benz(a)anthracene
chrvsene
3,3--dichlorobenzidine
bis(Z-ethvlhexvllohthalate
di-n--0etvl ohthalate
benzo(b)fluoranthene
D
I
I
I
I
I
I
benzo(k)fluoranthene
benzo(a)nvrene
i ndeno ( 1 2 3-cd' nvrene
dibenzo(a.h)anthracene
benzo(a h i '=rvlene
aniline
benzoic acid
benzvl alcohol
4-ch 1 oroan i 1 i ne
dibenzofuran
2..,rethvlnaohthalene
2..,rethvlohenol
4..,rethvlohenol
2 nitroa.niline
3 nitroa.nillne
4-nitroa.riiline
2,4 5-trichloroohenol
J -Estimated value.
STATE LABORATORY Of PUBLIC HEALTH
P.O. BOX 28047 -306 N. 1/ILHINGTON, ST., RALEIGH, N.C. 27611
ORGANIC rnEH[CAL ANALYSIS
LAB IIO '-77 ::?<./ 70 ...,., , ,V 7 / q 7 ::/<,/7,;)... ,:::,,7; y /'1
FIELD# ,!Jo -;J.i.i, .::Jo3fb:,, ,Jo, {C/7 .Jo-:<1x
TYPE ( '?) ( ~l ( :::1 ( . • l
UNITS .. ,. /ka ,,-,.,.,/.,n/ka ,/ /ka ,....-r .. n/ka
Jo/ •:io IA.--.. -I , " ,,,.<o l.'>n,
JOI '30
I
.I,
~L."O ,S()I
llo/330
IO/.J.:,o
soh1.<o
, I I I
\ '/ ' I '
l.'f O I, 1-"O I -I I , I ,
... ,
1a IZ-<n
~/
s-ot,l.,o
I I , ,
~, \ " ' .
m1H ..
H.a.OI Sall...
to be less than value given.
'7 /:; .. />~
;;)o...,. i/9
r. "",1
,,,.,.,..... ua/ka ,,.
J ' ,
,,
I
' I
It
I
K -Actual value is known
L -Actual value is known
u -Katerial was analyzed
NA -Not analyzed.
to be greater than value glven.
for but not detected. The nurt>er is the Minim..rn Detection Limit.
1/ -Tentative identification.
~/ -On NIU)C List of Priority Pollutants.
I
9',~ ✓-7\
,.:Jo: S-0 ' : ' --~ ··"/ka)
,
'
I ' .
✓
' ,
I STATE LABORATORY OF PUBLIC HEALTH
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC QjEHICAL ANALYSIS
/NEUTRAL ANO ACID LAB NO IU'7.-/ (/""1/, <-f7~VT7 ,'. ,ry ..,. /. 7r, 10 ./. .. 7'<../ V /" J C, ,,.., VP/
3o: -.:-I d<_o a .--i --,o-: "~ .,.?o -7 :.::J(J.:l\-:5 ..::io-i :TT,-,, EXTRACT ABLES FIELD# '-,
I COMPOUND TYPE (. ; \ ( ; \ ( : \ ( . <l ( I 71 ( '"7'1
UNITS ·= "n/kn .~.·-/k" ,.,.J.J, .. n/kn um':W"" u a/ k a .,-,..,ti, .. nlkn ·tmttfua/ka )
N nitrosodimethvlamine '" / :r:ro IA..-I , -I ~-IA I , I A
~ ·• (2-ch loroethvl lether
~ hlornnhenol
nt1enol t
1-<lichlorobenzene ' /
-dichlorobenzene L, ~~
I -<lichlorobenzene u
bi s(2-chloroi s:mrnnvl I ether nach I oroethane
i troso-<li -n...nrnnvl amine
nitrobenzene I ,ohorone
itrnnhenol
2. -<limethvlohenol
(2-chloroethoxvlmethane
; -<lichloroohenol ,,.
.4-trichlorobenzene ' na hthalene -~ :::i.01::· -achlorobutadiene A
h loro--m-creso l
he hlorocvclnn<>ntadiene
trichloroohenol
hloronaohthalene
acenaohthvlene
"'thvl ohthalate
; -<linitrotoluene
naohthene
2 4-dinitrf"V"'lhenol SQhfoSO
-<linitrotoluene I0/330
itr('V)henol .,oh,.-:o
fluorene /0/:130
: hlornnhenvlohenvlether
' •thvl ohthalate .I
-dinitro--o-cresol ,,,_,o SOI
~nvlamine /01330
nzene
·mnohenv l ohenv I ether
hexachlorobenzene ~ ,,
tachlornnhenol so/11,,s-o .
nanthrene ,,,, r:n0 ::i ~Qi-"
anthracene -3ov
utvl ohthalate I , / / / IA..
oranthene ~, \ \ I ,7 \ ' / 1..J./A .,
m"D L
'
Estimated value. H,.o/SO/ l-
Actual value is known to be less than value given.
• Actual value is known to be greater than value given.
U -Material was analyzed for but not detected. The nurber
I -Not analyzed.
-Tentative identification. -On NRDC List of Priority Pollutants.
is the HinirruTI Detection Limit. m"])L ----
I
I ..
I
I
BASE/NEUTRAL ANO ACID
EXTRACT ABLES
COl1POOND
nvrene
benzidine
0
I
I
I ,
I
I
I
I
I
butvl benzvl ohthalate
benz(a)anthracene
chrvsene
3 3-dichlorobenzidine
bis(Z-,,thvlhexvllnhthalate
di-n-octvl ohthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)ovrene
indeno(I 2 3-cd)nvrene
dibenzo(a h)anthracene
benzo(91h i l=rvlene
aniline
benzoic acid
benzvl alcohol
4--ch 1 oroan i l i ne
dibenzofuran
2-methvlnaohthalene
2--<rethvl oheno 1
4--<rethv 1 oheno 1
2 nitroani line
3 nitroanillne
4-nitroaniline
2 4 5 trichlo~henol
J -Estimated value.
STATE LABOAATORY Of PUBLIC HEALTH
P.O. BOX 28047 -306 N. ll!LHINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
LAB NO C,/ / "'i'/7(,-, ~i./ 77 lly-< .., ;,:;v7,Y "7~<./ /'1
FIELD # ~?o; ,-, .Jo: . .._-...J_ .-:21) ::i. ,:;i ;:?o":::?.~
TYPE ( ... ) ( ; ) ( ~) ( -:>, \
UNITS " ·-/l(n LI
-~,/ /kal · ,~.,.,_,.;,a/kn ,,, /kn
/0/~30 I,(__. lA-IA.-A
--1 ... c-0
/0/330
.I,
.so/lh,;O
I0/330
I0/.1.:?o
so/11;,,;-(J
, I / / /
l / I ' ' '
<oln.i:-o I.(__ iA-l ~ -vL-
.. ✓
/() /+111
..,,
sol,l.<;o
, / , / ,, ' ' ' ,
/')'11)L.
H:a.0/ $()It..
to be less than value given.
1'7 ,,~uy17 ..
' ' r 7'i
'11' .. :../k-
IA-
,
'
LA-
; . /
It
I
K -Actual value is known
L -Actual value is knQl,ln
U -Material was analyzed
NA -Not analyzed.
to be greater than value given.
for but not detected. The nurr,er is the Minirrun Detection Limit.
1/ -Tentative identification.
~/ -On NROC List of Priority Pollutants.
I
C/7-?i:/9/
,;;20-=?5-7-
( ""7\ -,,, ··"/kn l
;:.::.01:e
i,L
"'·c;oo , . ,
,
\I
I 7~7 ,
.,(_
,
' I
LA-
-
'
.--5 ok'
vL-
'-f ,~,~ 7
11,(_
,
\ 7
I STATE LABORATORY OF PUBLIC HEALTH
P.O. BOX 28047 -306 N. WILHINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEHICAL ANALYSIS
/NEUTRAL AND ACID LAB NO ~ "/'-fvY,'l 1'77,(r✓O::l 107:tiLYV ~-/,"'i -¥., <-r /-'$UY/-
EXTRACTABLES FIELD# ', ,., ..,--7 26~"9 ,;;;,=f ..;-q .J/J; ,,o ,?(}::? /, I
I TYPE ( '71 (r." l ( r7) ( r (. :a; l COHPOUND • .,..,,....-; • n i k a . '·-~ /ka ,,.,,,.,,...-"n /kn'\ , m-t:Y unlkn UNITS ,nfka
N-nitrosodimethvlamine ,,,,_,.,.o IA " IA -I A. -
b. (2 chloroethvl)ether
2 hlornnhenol ,
phenol I . I ,
~ -dichlorobenzene I ' ~-OIC
-dichlorobenzene 3 2,-,J,,· :::{ -:zo k.' i oC,,,
-dichlorobenzene IA--:2-::Z,-,J.-o ·,~~,11(-
bis(2-chloroisoornnvllether I . I A.
h achloroethane
itroso-di-n .nrl'V'\vlamine
nitrobenzene
i horone
itrmhenol
2 4-dimethvl oheno 1
(2-chloroethoxvlmethane
-dichlo~henol I /
.. 4-trichlorobenzene ' ~ I'
na>hthalene :2. oJ..• ·.:? -OY
ttl achlorobutadiene • A LA-'
l! h 1 oro-fil-Creso 1
he hlorocvcl=ntadiene
trichlornnhenol
hloronaphthalene .
acenaohthvlene
lthvl phthalate
-dinitrotoluene
naohthene
·ff-dinitrmhenol so/11oso
. -dinitrotoluene 101.,r.~o
i troohenol .,o/,,_co
fl uorene /0/:130
h--hlornnhenvlphenvlether I
.lll>thvl ohthalate .I.,
4 6-dinitro-o-cresol $0111,,,..lii.l
lnvlamine /0/330
nzene
r~henvlohenvlether
hexachlorobenzene ~ I r /
!11,tachlornnhenol so/11,,s-o ' \' ' ll~nanthrene I/I I' ,,0 '::? ::z ,., ,... :;cf -or ~30K.
anthracene . :? ~-") J,-'/ ~~ ,-,.J-,· ~ ~3,-,y'
ttutvl ohthalate u.-' , ,~ 1,(.--
oranthene \ ,.;., /11?/J ~,'r) Q-=!::.: /,2.00 ,,,
m1)L , ,
Estimated value. f{.,_O/SO/L-
Actual value is known to be less than value given.
Actual value is known to ·be-greater than value given.
U -Haterial was analyzed for but not detected, The nurt>er is the Hinirrun Detection Limit. mIJL ---E -Not analyzed.
-Tentative identification.
_ -On NRDC List of Priority Pollutants.
-
IC/7-< c/ ,Y7
.2/>-/,, .1.
( ·. ') .. ,nfkn ')
I -
,
'
I
••
I BASE/NEUTRAL ANO ACID
EXTRACTABLES
I
I
I
n
COHPOONO
ovrene
benzidine
butyl benzyl phthalate
benz(a)anthracene
chrvsene
3 3-<1ichlorobenzidine
bis (2-ethvl hexyl) phtha 1 ate
di-n-octvl ohthalate
benzo(blfluoranthene
benzo(k)fluoranthene
benzo(a)nvrene
i ndeno ( 1 . 2 3-cd) nvrene
dibenzo(a.h)anthracene
benzo(q h, i )n<>rylene
aniline
benzoic acid
benzvl a 1 coho 1
4-ch 1 a roan i 1 i ne
dibenzofuran
2-<nethvlnaohthalene
2-<nethylphenol
4-<nethv 1 oheno 1
2 nitre.aniline
3-nitroaniline
4--nitroaniline
2 4.5-trichlorooh<enol
J -Estimated value.
STATE LABOAATORY Of PUBLIC HEALTH
· P.O. BOX 28047 -306 N. ~!LM!NGTON, 51., RALE[GH, N.C. 21611
ORGANIC CHEHlCAL ANALYSlS
LAB NO ..,, 'l ~ rLJY} 4'7• rir f? -1 C, 7 :7</J'/..1 C..,-"7 -(l•,Y."l
FIELD # ,.7 /f; i,; '7 ~o: t.,, .V ,.::, 0 -'S ,-., .:J1-,. l/,n
TYPE ( , 7') • ( ; ) ( '7) ( . ·1
UNITS ~ .. n/ka ·---•. ,a/kn ., /kn . ..-u 110/kn J
/0/~:in '7 ::,-r. . . ~ .,,,,~ /,U ~~ ..-n /,,,.,:;o 'v<-L -A. -
·~ I~ -
/0/330 /,,,7 ::1::1·-1 ~v;i,;;z ;.. ./A/,,,7 RIOOO ·~ l. ,I ,c_ , • ,t
. r , ,. I
'It. -:o SO/ ,J' ,v ' 'I
Jo/330 Y-/4 /4 /4,; i~ _Q1)n :;;/ J _/1/10 I 2.'J ,-.1. 7
/O/.J3o (L-, . ,I ,. . . ,.,,
so/,.,,,;o
/ / / r
,/ \ ' \
<o/Jt..~O // r,L_ A-t ,L__
... ,,,. r I
IOI.BO ' I \
I ,{. 01c :a; . ov
' LA--IA-
,J,. II tJOO
s-ot,1_,:;o 'A
/ ,
\/ I ' I • I "
I
mn1-
H:a.ol Sa/L
to be less than value given.
o/7 ~<;t,P/,.,
.:J17~/,./
( ·; '\
'· -"uo/kn -
, .
,,~ 700 :,
/
'
.,
I
'
I
i'
I
I
I
I
I
I
I,
I
I
K -Actual value ls kO<Jl',ln
L -Actual value ls known
U -Material was analyzed
NA -Not dnalyzed.
to be greater than va 1 ue g.i ven.
for but not detected. The nurbcr 1s the Hinirrun Detection Limit.
1/ -Tentative identification.
~/ -On NROC List of Priority Pollutants.
1(/,V/ q7;i
"o:. 7.-,
,: ' \
• ....-••0 /ka 1
u_.
,.
\
'TOO
1,1___.
7
\
v<.__
/
\
I STATE LABORATORY OF PUBLIC HEALTH
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
/NEUTRAL AND ACID LAB NO 10-/-rY-AA fQ?:?VP'-1 t:r, :-< vqo Q7 -1 '/'11 .
7 ,';)... , .,
EXTRACTABLES FIELD -~, ... ::i ,,_ ~ 1~ ;;i.,_ <.I ~o::l.1~, ....;,o ,. .26-V-7 # ,
( ,< l (_3 l (3) ' ::, ) ( -) COHPOOND TYPE
UNITS -.. ~ .... -;kn -,,,,,. -/kn1 ,... __ /kn ,_,,-,:,n/ka~ -I Y"" . -·'k-
N-nitrosodimethvlamine fr.l;/"10 v-.-I ,, iA-IA -
1(2-ch loroethvl )ether
hlornnhenol
nol j 3-dichlorobenzene
4-dichlorobenzene
2-dichlorobenzene
bis(2-chloroisonrnnvl)ether
ach 1 oroethane
itroso-di -n--nrnnvlamine
nitrobenzene
·~horone
Jnitr(V'\henol
,4-dimethvlohenol
bis(2-chloroethoxvlmethane
14-dichloroohenol
2.4-trichlorobenzene
naphthalene
1xachlorobutadiene
ch 1 oro-m-creso l
he hlorocvclnnPntadiene . trichlornnhenol
chloronaohthalene
enaohthvlene
dimethyl ohthalate
16-dinitrotoluene
enaohthene
2.4-dinitrnnhenol SQ/1"1SO
4-dinitrotoluene l()l.'i~O
nitrnnhenol .,01 '·'-0
fluorene /0-' :l30
chlornnhenvlohenvlether
ethyl phtha late, .
6-dinitro-o-cresol so, ),-_,o
~nvlamine /0/330
nzene
·aooohenyl phenvl ether
hexachlorobenzene ~
tachlornnhenol so/16,:fO
nanthrene //1/ i.''?O
anthracene
ltvl ohthalate / / / I I'
oranthene \ , ' . \ \ , '\ I
m"'D L
'
Estimated value. H,.o/SO/L-
Actual value is known to be less than value given.
Actual value is known to be greater than value given.
U -Katerial was analyzed for but not detected. The nurber NA -Not analyzed.
1s the Mini1TU11 Detection Limit. mTJL ---I -Tentative ldentiflcation.
-.On NRDC List of Priority Pollutants.
I
.,~ . ,'~ -, .,n 'l-O
(~ ,. /ko l
IA._;;;
r
'I
~ ~Ok:.
?./C,,7
;;c~0 ,;..
vL.-
-' -(, 7 ,,,__
/
'\
"j()O
L.i.t. 7
l,A--
~.1./00 ,
I
•• I BASE/NEUTRAL ANO ACID
EXTRACT ABLES
I
I
I
I
u
D
If'
I
I
I
I
CD1POONO
nvrene
benzidine
butvl ben,vl ohthalate
benz(a)anthracene
chrvsene
3 3-dichlorobenzidine
bis(2-ethvlhexvllohthalate
di n-octvl ohthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(alnvrene
i ndeno ( I 2 3-<:d \ ovrene
dibenzo(a h)anthracene
benzo(a h i l=rvlene
aniline
benzoi c acid
benzvl a lcoho 1
4-<:h 1 oroan i 1 i ne
dibenzofuran
2-methvlnaohthalene
2-methvlohenol
4-methvlohenol
2-nitroaniline
3-nltroani 1 ine
4-nitroaniline
2.4 5 trichloroohenol
J -Estimated value.
STATE LABOAATOOY Of PUBLIC HEALlH
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 21611
ORGANIC CHEMICAL ANALYSIS
LAB NO -, /. :,c/,Y J <-/7-?<J.r, / ./ Y,O .., /-'l7-//
FIELD# .:?o =-,,,_ ,{ -,-)/,J ..2.0. ;;/(;, J . .J o-.:?1,,, I' A
TYPE ( -11 ( . ) (~) ( 2.'
UNITS ·-~1.,,,n/ka • ~ /ko · ,.,,. 10/kn ~ /k~
/0/~'?0 u_ ,,.____ IA A -
,,, i,,.<o
/0/330
.I,
so/N .. -ro
lo/330
I0/.1.::/o
so/1"50
/ / I I'
' / \ ' ' '
<" 0 h,.. ... 0 l,.A-I • ·~ ')
' ,
ia z=r.:ui
,,.
s-o/,l..<:o
/ / / / ._, ' \ ' \
n,1)1..
H2.0I Sall..
to be less thdn value given.
(i)
..., ✓ .... ,., , c/ 7 .,a;,:; -<
;,20'<(,,"7 ,:;f,j_;i?,;r,
( -,, ' ('"7"\
.. ,,. /kn ua/ko""\
LI\.... 4/C~ ,, ~
/
~· .?.:l~ ,
/ /
'\ '
IA -I' .
,
\
I., .. 7
(.A..-
'27/ ''7
.
/ . .
I,
I
K -Actual value is known
L -ActUdl value is known
U -'1aterial was analyzed
NA -Not analyzed.
to be greater than value given.
for but not detected. The nurber 1s the Hinirn..m Detection Limit.
1/ -Tentative identification.
~/ -On NROC List of Priority Pollutants.
'NCDE;lNR
· !)ivision of Wnstc Management /!J Superfund Sectiou
□ Hazardous Waste Section g • 0 Solid Waste Scctiou OCT 211997
SUPERFUND SECTION CHAIN OF CUSTODY RECORD D
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Project Name: Sr'~(YlcJ/75 ~'c_ 7Zl,dc.-Sampled By: lX>/lr""--()_;r'/-;,o"Y\
Site ID # (NCD#) N L-{J a, Z-5s_:;; 7q Z-Sampler ID
Location: S-faf-e;,,,/ I I c., /VC Telephone:(16) 7 3'3-7.JoO/ qd 3i7 Address: 17.,(,, 'i3 c,J-h, / ;,__ !Zd-Date Sampled: -aL z:s£ t/1 , cz,l_u,(11
' ' Time Sampled:
Sample Types: Soil \Yater v-Waste Other
Remarks: pH c_e~ues fe-d Q/\ sa yle.s <}70l,./f\ be( QUJ w(-f/n a_[,f('r//e,_
Ct?,/ { g f0'11d2 UJtl f-v-) . U /\ cc C, "dr'AcJ Cdt!;.o/e.. for 1!.H +es n ['j-wl{(
L~br ✓ be.. 'O &f tt./.11 e cl -iYot1t.1 or ,,-al"\ r'CS .J
Field Sample *on '"Z->'J IF"o17 7-(j,o 1ro17u / ,,c O(] -ZbZ-"017ZJ,,3 ~0(7 7.C:,C(-0(7 Z6 s: Numbers or7·U,G, 0(77_;;,7 0/7Z..&8 0/ 7'2[,,'1 of77-7o o/7Z-7/ 11'6 /]?. 7Z...
of]7-7 3, b ( TZ-74-tc o f7 7... 7.S I0(71-7b :ro/7.1,,7.1
Relinquished By': h\i IA~ \. 1 r1 /;,/cr,1....--Date: #Z-'?J.12]_ Time: 3 '. 05
(Sienatmc) (
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, A -
Received By: /#/(U / ,£/4 p?'p( Date~,y: 2r Time: -:J_, --·O f G(signature) --.
Relinquished By: Date: Time: (SiPnaturc)
Received By: Date: Time:
(Signature)
Relinquished By: Date: Time:
(~ionaturc l
Received By: Date: Time:
(Signature)
A / .
Results Reported: _dt/ f:/ //4/,·/ /L_ Date: 11tJe,T't_?-Time:
(Sign;turc) V . ,_.
' 'NCDEHNR I J?ivision of Waste Management
-el-Superfund Section
Organics Lab: --Inorganics Lab: V
C Hazardous Waste Section
.. D Solid Waste Section
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CHAIN OF CUSTODY RECORD
Project Name: Sr~(Ylu/75 $f'b'c ;ZL,dc.-Sampled By: ex:,,, fl"\_, ()Jr' Is.on.
Site ID # (NCD#) N l-/) Ob 2-5~ 7q Z-'Sampler ID
Location: ,s1;A,hv i I 7 c., /\JC. Telephone:(WJ 7 33-7,€0/ fy{-317 Address: l?.fc, '3 ty.fr,/;..__ {2d. Date Sampled: <B/2-s/17 , q,[u;(C/1
' Time Sampled:
Sample Types: Soil 1..,./' Water Waste V Other
Remarks: 5!1¥,:(e.S. inJi·~-cJ t,,Jt' ~ tts-kc I lc._ cue... U--1tsbz-121'/)&.u_J Ci."d ...,.s.+, 1"'-' (C-=,t'&.e<\-h'ocl ~~ -s.C.,~ -Si)_ey/e..s I /'\cU=--+e ~ L.Vi t/A J,ouk,/e.. <l.S,.+<"ri /L J
tJ.r e. Soi I (l_ rd L-<»-'.:.tL ~,odu. c.t .
Field Sample Of7·Z-76 ot7-Z. ]j 0/12.fu 0(77..'?:,/ 0[17..>oZ-O/T23~ 0(77-<c:1-
Numbers onz.fJC Ol7 ?.6b or7-z.q,,*'o17-z..<c,8 ~/7?-?!) 'k 0(7 -z,qo ,)\c-o I 7 ?f( (
.at-<D I? -z.q -,__ 'lr-or7-zq3 or7ZJ?f 0/7?."l.i 0{77.q{. 0(7'2.'J..7 t>/727'i
on2-11 o I T~oo ~ o/730/
Relinquished Byl Pr!1 l,u,-\....._) () i!,'PSp,-.. Date: '2/VV/47 Time: 3,a;
/Sionatur""--' U ,
Received By: ~-,,---,, &/4/~ Date:~-:)'-~Time:'3"<::) ,r-__,. :.--""f -
(Signature)
Relinquished By: . Date: Time:
/Sionature1
Received By: Date: Time:
(Signature)
Relinquished By: Date: Time: r.~iPnaturc)
Received By: Date: Time:
(Signat~r'.;} £.. , / ,
Results Reported: 1,/M'-:;' //4-1/ // ffp Date:/,C/}_,ttf. t--Time: (Sig,1aturc) -
V I •NCDEHNR
Divis· of Waste Mairngcmcnt
uperfund Section
Organics Lab: -------c-lnorganics Lab: L.---'
□ Hazardous Waste Section
--□ Solid Waste Section
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CHAIN OF CUSTODY RECORD
Sampled By: ,~ tJ,/son
Sampler ID __________ _
Telephone:(__) 23'.?-2~0/ x s.J 7
Date Sampled: 6)26/J 7~ /
Time Sampled: ____ · ______ _
Sample Types: Soil ---Water ~-Waste __ _ Other ---
Field Sample
Numbers
h/7 3DZ
0/73~
0 /770 t,I
t?/731/ ---------o 17:?<;,J.,
C2L13iZJ
ot7~.Jft
0/7310
Received By: 9 °'i ~., ~a.,..;..,_,
(Signature)
Relinquished By: --------------Si nature
Received By: ---------------
(Signature)
Date:E!>}~<t/'97 Tirne: __ 1_1'.1/s!.
Date: Time: ----
Date: Time: --------
D Relinquished By: _____________ _
Si nature
Date: ----Time: ----
Received By: ---------------Date: ----Time: 0 (Signature) .
Results Reported :_£,(&.'._f:;~41,~~~".':::::=::::::____ 1W (Signature)
Date: /J?Jef'f,r Time: __ _
E
I 'N.C. Ocpartmcnl of l:1win,..ir ... 1,·,
\ lcalth, & Natural Resources
Solid Waste Management Oivisiou
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Dox 28047, 306 N. Wiimington Street
Raleigh, Nerti\ Carolina 27611
•• , Number_cM_:__c,::_c.,""0~C0--".C..:L=-'-_ __c~-,.c..:-s_c:5_~-'-./_,_'1_Z.. ___ Field Sample Number DI] Z-7 'i3
Name of Site S(jrno/1 S 4kc... ffi/1/c.. Site Location S/qjcy //I'( /e_
I Collected By j 5 ID# ___ Date Collected Cc, (2.S{ q7 Time_,..,/S=--Z.U-=--
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Agency: Hazardous Waste Solid Waste Vs u perfund
--
Sample Type
EnYironmental Concentrate Comments
__ Groundwater (1) Solid (5) Sedr'me,"' +, be/ow' ,
__ Surface water (2) Liquid (6) PPG
✓ Soil (3) Sludge (7) <;,S-o, -Si)
. Other ( 4) _ Other (8)
Organic Chemistry Inorganic Chemistry
Parameter Results(mg/1) Parameter Resul' :t ... ('11g/kg)
P&T:GC/MS V Arsenic L.. 'i ---
Ac;d:E/N Ext. ✓Barium so
.. ,MTllE VCadmi.im L.. \0 ----Chloride ----V Chromium 40 .
--
--__ Copper
Fluoride ----Iron -----
--i,_,,,-Lead L_ \(')
--v Manganese .500
--~ Mercury L_ D _D ":f
Nitrate ----v Selenium -<C. .J.
V Silver L..' C)
Radiochemistry --Sulfates
······-.. Zinc --l•arametcr Results (PCi/1) _pH
__ Gross Alpha --Conductivity
Gross Beta TDS ----TOC --·-·-·· --
Microbiology --
--Parameter Results (Col/lOOml) -------
----
. ----
Date Received Reported by .
Dale ExtractcJ Date Reported
012f37 AUG 25 97
Dale Analyzed Lab Number . '" ' .. ~. ". ; " ' ... ,,,,,
TCLP Compounds
Inorganic Compounds Kesu,ts(mg/1)
Arsenic --Barium --Cadmium, --Chromium --Lead --__ Mercury
Selenium --Silver --
--
--
--
--
Organic Compounds Resnlts(mg/1)
benzene --carb0r. tetra.:hi0ricie --chlordane --chlorobcnzenc --chloroform --o•cresol --n:-creso: --__ p-crcsol
cresol --1, 4-dichlor0benzene --1,2-dichloroethane ----1, 1-dichloroethylene
2,4-dinitrotoluene --
--heptachlor
hexachlorobenzene --hexachlorobut adicne --hexachloroethane
__ methyl etl1yl ketone
n.itrobcn::ene --__ pentachloroµ~1enoi
__ pyridine
__ tetrachloroethylene
__ trichlocoethylece
__ 2,4,5-trichlorophenoi
__ 2,4,6-trichlorophenol
__ vinyl chloride . ,.• -·. . .
endrin --lindanc --__ methoxychlor
__ toxaphcne
2,4-D --2,4,5-TP (Silvex)
--
I 'N.C. Dcpanmcnt of Environment,
I lcallh, & Natural Rcso.irccs
Solid Waste Management Division
SA..l\1PLE ANALYSIS REQUEST State Laboratory of Public Health
P. 0. Box 28047, 306 N. Wilmir.gton Street
Rlllcig.h, North CarolinJa 27611
I. Number NCU C0 Z-Field Sample Number 0(72 7'7
Namc of Site Stjtno/1 S S!(-kc...
I CoHected By j S
Site Location Sfqfcy Vi/ /e__
ID# ___ Date Collected f3 ( 'l.S ( q1 Time / 1--10
I Agency: Hazardous Waste Solid Waste Vs u perfund
Sample Type
I E11vironmcntal Concentrate Comments
__ Ground water (1) Solid (5)
I
:::,e &.i me,'\,+1 ~clc='jTO.."°
__ Surface water (2) _Liquid (6) :p0'\il
I _IL_ Soil (3) Sludge (7)
_ Other (4) __ Other (8\
g
Organic Chemistry Inorganic Chemistry
D Parame~er Results(mi/li Parametfr
_J.c_ Arsenic
_____!L Earium
Result ♦ g¢, (•ng/kg)
;>&--:-:GC/MS --= Acid:B/N Ext. ur-MTl:iE
---E --
--
--
I --
--
--
--
V Cadmium
--Chloride
_iL:. Chromium
__ Copper
Flu0ridc
JrOL
v Lead
V .Manganese
V Mercury
Nitrate I . l., Selenium
----------------' V Silver
Radiochemistry
I · ;;;,;·ameter Results (PCi/1)
__ Gross Alpha I __ Gross Bela -------
--
Sulfates
Zinc
_pH
__ Conductivity
TDS --TOC
1 Microbiology
■1~------l __
~meter Results (Col/lOOml)
'1
.L. 'J.O
L... ,o
Ji:j
.,_ \D
30
I Dale Received ________ Reported by ___ -'-------
Dale Exlraclcu Dale Rcnorled
I ----·01·~21~38~AU~G2~89~7~-
Date Analy1.eu Lab Number
1\11<..' 'Ill)\ /lln.,:,.,,,j "}/111\ ----------
TCLP Compounds
Ino~anic Compounds
Arsenic
Barium --Cadmium,
Chromium --Lead
__ Mercury
Selenium
Silver
Resul,s(mg/:)
----------------.,
O~anlc Compounds Rrsults(mg_i:J
benzene --carbon tetrachlorid~ --chlordane --chlorobcnzene --chloroform --o-cresoi --m-cresol ----p-cresol
cresol .----:,4-dichlorobcnzcne _____ _
1,2-dichloroethane
__ 1,1-dichloroethylene ______ _
__ 2,4-dinitrotoluene
__ heptachlor
hcxachlorobenzene
. hexachlorobutadicne ---------hexachloroethane
__ methyl ethyl keton~ _____ _
riitrobe·nzcne
--pcntachl0rop\;eno:
__ pyridine
__ tetrachloroethylene
__ trichloroethylene
__ 2,4,5-trichlorophenol . ------__ 2,4,6-trichlorophenol _____ _
__ vinyl chloride
endrin
lindanc ----melhoxychlor
__ toxaphcne
_2,4-0
_ 2,4,5-TP (Silvcx)
I '1''.C. Ocpanment of Environment,
I lcalth, & Nalura\ Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
sss 7C/2-. Fieid Sample Number
State Laboratory o~ Public Health
P.O. Dox 28047, 305 l\. Wilmington Street
Raleigh, North Carolina 27611
O /7Z-0o •• Number Alco C0 z__
S14s //( //e__ Name of Site C_/ I Set?n'c... 7it/l/C.. Site Location -:3rno//.S I Collected By 0S ID# Dale Collected fd_-zslci1 Time (3/S
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds
----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
S eJ.\ ',1rx er,+ Barium --
· __ Ground water (1) Solid (5) Cadmium, --
I P211~uJ s.±WM
Chromium --
__ Surface water (2) _ Liquid (6) Lead --Mercury
ss-09-sD --
I V Soil (3) _ Sludge (7) Selenium --Silver --
_ Other (4) _ Other (8) --
m
--
. ---
Organic Chemistry Inorganic Chemistry --
m Purnmcier Results(mg/1) Parameter Results~(mg/kg) Organic Compounds Results(mg/1)
_ P&T:GC/MS L-Anenic <4 benzene
', --
Acid:B/N Ext. v Bariuci ,~o carbon tetrachloride --
0 MTBE V Cadmium L.iO chlordane ------
Chloride chlorobenzenc ------
C/ ChromiulT'. \ (_., chloroform ------
D --Coppe_. o-cresol ----.. , .. _ Fluoride m-cresol ------
--· iron __ p-cresol
n ---v -Lead L_ \('I cresol
.,. .. ----
--~ Manganese ~~o --1,4-dichlorobcnzene
--_i,c_ Mercury .L. D -°J --1,2-dichlorocthane
--Nitrate __ 1,1-dichloroethylene
E V Selenium ,Cl 2, 4-dinitrotoluene
t/ Silver
--
L__ \0 . __ . heptachlor --
Radiochemistry Sulfates hc:xachlo.r_qlJenzene
m
----
······-··---Zinc . hexachlorobutadiene
Parameter Results (PCi/1) ----
_pH hexach!oroethane --
__ Gross Alpha _· _ Conductivity __ methyl ethyl ketone
m Gross Beta TDS ni~robenzcne ------
TOC __ pentachlorophenol --
--__ pyridine
I Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --
I
lindane
Date Received
--
Reported by __ melhoxychlor
__ toxaphene
D:ilc Extracted Date Reraf~ 2,4-0
I --139 AUG 2897 _ 2,4,5-TP (Silvex)
Date An:ily1ed Lab Number --
1)11<.: 111)1 (11,-.viu•rl ?/()1,
I N.C. Department of Environment,
I lcahh, & Nalura\ Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State IJ1boratory of Public Health
P.O. Box ~7, 306 l\'." Wi!mington Street
Raleigh, North Carolina 27611
.. Number Alco or; 2--S"S5 712-. Field Sample Numbe. 6 (7 Z ZJ /
· Name of Site '-fjri'I0/1 S yt'-h'c... ?a,;1/c.. Site Location Sfq}eyvr //e_
I Collectc·d By-=l--'-""--J:>.:.C(=:./~u1=,:___;_-=-_,ID-=#::==~-Date Collected eo(rz<o( en Time o94s
I Agency: Hazardous Waste Solid Waste Vsuperfund
I Sample Type
Environmental Concentrate Comments
Ground water (1)
I = Surface water (2)
_ Solid (5;
_ Liquid (6) _,l)=-tW------'---i~=~=--1"-Po=/\=J,_· __
I 'v Soil (3)
_ Other (4)
-Sludge (7) _-----'s"-'s=---L...:O=-·--=S,=-->DJ-----
-Other (8) ___________ _
Organic Chemistry lno,·ganic Chemistry
Results(mg/1) Parameter Results ....... (mg/kg)
_ P&:T:GC/MS 1.,.../"" Ars.;:fuc L.3 9
Acid: B /N Ext. i V Bar,mn cl 0
MTBE V Cadmiull' "'-'1.8
Chlnride
v_ Ch,omiun: \:J,
--Copper
F:uoride
Iron --
..J./ _ Lead .!..9.r,
_:::=_ Manganese ~7 ~ Mercury L.z::,dc,9
Nitrate --V Selenium .L..;),
✓· Silver -<:.9.'o
Radiochemistry Sulfates
Zinc
Pani111etcr Results (PCi/1) pH
__ Gross Alpha __ Cc,nductivily
Gross Bela TDS
TOC
Microbiology
Parameter Results (Col/lOOrr.l)
I Date Received Reported by
I Dale ExlracleJ Dale Rer,orted 01~140 AOC 2897
Dale Analyzed Lab Number
""'' ~"" ,,,_.
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium·
Chromium
Lead
Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobcnzene
chloroform
o-cresol
m-cresol
__ p-cresol
cresol
1,4-dichlorobenzcne
1,2-dichlorocthane
1, 1-dichloroethylcne
2,4-dinitrotoluene
heplachlor
hexach lorobenzene
. hexachlorobutadiene
hexachloroethanc
__ methyl ethyl ketone
nitrober,zcne
__ penlachlorophenol
__ pyridine
telrachloroethylene
__ trichloroethylene
__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol
__ vinyl chloride
endrin
lindane
__ melhoxychlor
__ toxarhcne
2,4-D
_ 2,4,5-TP (Silvex)
Results(mg/1)
Results(mg/1)
I N.C. Department of Environment,
1 lcnllh, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory or Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
lee Number /VC,Q Ct;; 2--SS.S 7'1 Z... Field Sample, Number . 0 (7 2-'6 ?-
Name of Site S;3mo/l S Stf-kc... 72!.;t /c.. Site Location Sf q.}ey VI '//e..
I Collected By JS ID# ___ Date Collected 0(71p( 41 Time {3oG
I Agency: Hazardous Waste Solid Waste Vsuperfund
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Sample Type
Environmental Concentrate Comments
__ Ground water (1) _ Solid (5)
__ Surface water (2) _Liquid (6)
V Soil (3). _ Sludge (7)
_ Other (4) _ Other (8)
Organic Chemistry Inorganic Chemistry
_ P&T:GC/MS
Acid: B /N Ext.
MTIJE
Resul!s(mg/1) Parameter
L/" An,enic
v Ba:;ium
V Cadmium
Chloride
v Chrorr:ium
__ Copper
· Fluoride
Iron
'-' Lead
J.... o_ c"I •t---------4
__::::::_ Manganese
_i::::..Mercury
Nitrate
v Selenium
V Silver
Sulfates
L, 10
I
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Radiochemistry
Parameter
__ Gross Alpha
Gross Beta
Results (PCi/1)
Zinc
_pH
__ Conductivity
TDS
TOC
I Microbiology
1~-----1
Parameter Results (Col/lOOml)
I Date Received ________ Reported by _________ _
Date Ext,actcJ Date Reported ·
I ----01rr.21.--.4r.r1~Au=c""""2s=9=7-
l)a1c AnalyLc<l Lab Number
\\I 1<..: 1.1<11 ru,..,,;,.,..,l 1101\ ----------
TCLP Compounds
Inorganic Com pounds
Arsenic
Barium
Cadmium,
ChromiuIT'.
I.,ead
__ Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-creso!
m-creso:
__ p-cresol
cresol
1,4-dichlorobcnzene
1,2-dichloroethane
Results(mg/1)
Results(mg/1)
------
------
__ 1,1-dichloroethylene _____ _
2,4-dinitrotoluene
__ heptachlor
hexachlorobenzene
hexachlorobutadiene
1.exachloroethane
methyl ethyl ketone
nitrobcnzcne
__ pentach,orophenol
__ pyridine
__ tetrachloroethylene
__ trichloroethylene ·
_· _2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol
__ vinyl chloride
endrin
lindanc
__ methoxychlor
toxaphene
2,4-D
__ 2,4,5-TP (Silvcx)
------
(1-N.C. Ocpanment of Environment, ti I kalth, & Natural Resources
· Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Labon1tory c-f Public Health
P.O. box 28047, 306 N:Wilmington Street
Raleigh, North Carolina 27611
· lie, Number NCO Ct;; Z-SS5 71 Z.. Field Sample Number 0(7 Z 'G5
Name of Site S(jmo/1 S Stp-kc.... 7a,;1,/c.. Site Location Sf.:J.es Vi '//e__ I Collected By-'-4-'-"""-~'-'. ::C~--..=::::;:....c...:::__-1.ID-"-'>.#::==~-Date Collected <2>(z0 ( q, Time __ /_5_3'_.S __
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds
----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
C4 ~ u (\ J_
Barium --
__ Groundwater (1) _ Solid (5) Cadmium. --I __ Surface water (2)
Chromium
h:e.io,je.. c\,L~ --
_ Liquid (6) Lead --__ Mercury I V Soil (3) _ Sludge (7) ss-r~-sL Selenium --Silver --
_ Other (4) _ Other (8) --
I --
--
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Result,/ilf 't,(;cg/kg) Organic Compounds Kesults(mg/1)
_ P&T:GC/MS ~Arsenic :..:.. '-I benze~e
'cso --
Acid:B/N Ext. L/' Barium carbon tetrachloride
MTBE 1...--Cadmiom --
,!_ \0 chlordane ------Chloride chlorobenzene ------
V Chromium 18 chloroform ·-----I --·-Copper 0-cresol --
--Fluoride m-cresol -------
Iron __ p-cresol --
I --t/' Lead L.)Q cresol
v Manganese
--
--,;:).60 1,4-dichlorobenzene --v Mercury L.a.a9 --1,2-dichloroethane --
I --Nitrate __ 1,1-dichloroethylene --V Selenium "'-d, 2,4-dinitrotoluene --
l./ Silver .,/._ )(\ __ heptachlor --
I
Radiochemistry · Sulfates hexachlorobenzene ----
······-·· Zinc . hexachlorobutadicne
Param~ter Results (PCi/1) ----
_pH hexachloroethane --
I
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
--Gross Beta TDS nitrvbenzene ----TOC __ pentachlorophenol --__ p)Tidine --
I Microbiology --__ tetrachloroethylene
--__ trichlornethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
~ __ 2,4,6-trichlorophenol --
--__ ·. vinyl chloride
endrin --
lindane
I Date Received
--
Reported by __ methoxychlor
toxa;,hcne --
D,,tc ·Exlracle<l Dale Reported 2,4-D
I 012142 AUG 2697 --_ 2,4,5-TP (Silvcx)
Dale Analyzed Lab Number --
1,11, 1.1<n n1,..,,~,-d 11tJ1)
ft N.C. Dcpanmcnt of Environment, U I lcallh, & Natural Resources
Solid Waste Management OiVU:ion
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilrr.ington Street
Raleigh, North Carolina 27611
0.-, Number Alco Dr;; z_ s-S5 71 z.. Field Sample Number 6 (7 7-81--
Name of Site SJ3rno/l S 51'ii'c... 7a,;1/c.. Site wcation · Sfqfey /// / /e_
0 Collected By-~-'-"'c.:..j)=-vt,-,\--=+:--..c...::=----.1.ID-""-#::==~-Date Collected 'c{zs ( c,7 Time _ __,{~'o-=--'2.S __ _
0 Agency: Hazardous Waste Solid Waste Vsuperfund
Sample Type
Environmental Concentrate Comments
__ Ground water (1)
I __ Surface water (2)
_ Solid (5) ':::/'' cl~l'I\ e ,\+-
-Liquid (6) _4:-'-'-':.c.+_, _S~tr--'-'-'e;:..;_'Nv\-'--'-__ _
· • v Soil (3)
_ Other (4)
_ Sludge (1) l,(..;2, St ct. '.S,;'-\-..:..
_ Other (8) c;;,_S,,-/VS D
Organic Chemistry
Parameter
P&T:GC/MS
Acid:13/N Ext.
MTBE
Results(mg/1)
Inorganic Chemistry
Parameter
_k_ Arsenic
V Barium
i./ Cadmium
Chloride
v Chromium
__ Copper
Fluoride
Iron
L.-Lead
Results~(mg/kg)
L.").9
_::::... Manganese
_k_ Mercury
Nitrate
i,,, ·selenillm
,.___ Silver
Radiochemistry Sulfates I --------------4 Zinc
Parameter Results (PCi/1) __ pH
__ Gross Alpha Conductivity
Gross Beta TDS
TOC
Microbiology
Parameter Results (Col/lOOml)
I Date Rec·eivcd . Reported by _________ _
I IY:iie ExlractcJ ________ Dale Reported
012=1~43~A=uc~2~u 9=7~
Dale Analyzed Lab Number
'" ,. . .,,,., ,., ·--c,--c,c-.,,~"----------------
TCLP Compounds
Inorganic Com pounds
Arsenic
Barium
Cadmium•
Chromium
Lead
__ Mercury
Selenium
Silver
. Organic Compounds
benzene
carbon tetrachloride
chlordane
eh\orobenzene
chloroform
O-CT::!SO:
m-cresol
p-creso;
cresol
Resuits(mg/1)
Results(mg/1)
------
1,4-d:d:lorobenzcne _____ _
1,2-dichloroethane
1,1-diehloroethylene _____ _
__ · 2,4-dinitrotoiuene
__ heptachlor
hexachlorobenzene
hexachlorobutadiene
hexaehioroethane
__ methyl ethyl kelo!le
nitro!:>enzene
__ pentachloropheno!
__ pyridine
__ tetrachloroethylene
__ trichlorocthylene
__ 2,4,5-trichloropheno'
__ Z,4,6-triehlorophenol
__ vinyl chloride
endrin
lindane
methoxvehlor --,
toxaphene
2,4-D
_ 2,4,5-TP (Silvex)
------
0 N.C. Department of Environment,
I lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 I\'. Wilmington Street
Raleigh, North Carolina 27611
. U.e Number NCO 00 z_ sss 71 Z.. Field Sample Number 6 (7 z_ e,s
Name of Site_'y__,_JJ"'I' _rn"'o"'/l-=S=---=4='-fi_'-=c:...=---__,7a,...=c:...ll::..c/<_c:.. __ · Site Location Sfde,svr //e_.
m Collected By J 5, ID# ___ Date Collected '?J..'2£/ '17 Time [73,5
I Agency: Hazardous Waste Solid Waste Vsuperfund
Sample Type
I Environmental Concentrate Comments
__ Ground water (1)
I __ Surface water (2)
I V Soil (3)
_ Other (4)
_ Solid (5) '.:::e!tm?1\{-
-Liquid (6) ---'-Lu_/ .:..,.l ("'-ict_/Y\_S'=--rl"-· -'C-rn-'-ct-"-' --
-Sludge (7) __ SS,--_--'/-'1-~_S._· ·=D __ _
Other (8) __________ _
~-
,-------------+--------------1
Organic Chemistry Inorganic Chemistry
I
_P&T:GC/MS
Acid:B/N Ext.
MTBE
Results(mg/1) Parameter
v Arsenic
\...,'""'. Barium
v Cadmium
Chloride
[., Chron:.ium
__ Copper
Fluoride
Iron
i....-Lead
_.:::.. Manganese
v Mercury
Nitrate
c.-Selenium
'-"--'-~-----------< L--Silver
..t.. 9 .. R
Radiochemistry
I Parameter Results (PCi/1)
Sulfates
Zinc
_pH
I
I
__ Gross Alpha
Gross Beta
Microbiology
Parameter Results (Col/lOOml)
__ Conductivity
TDS
TOC
.Oate Received ________ Reported by _________ _
Dole Extractccl Date Repw\nl . . . ----UlL14¢ AUG2697
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium,
Chromium
Lead
__ Mercury
Selenium
Silver
Organic Compounds
benzene
carbor. tctrachloricie
Results(mg/1)
Results(mg/1)
------chlordane
chlorobenzene
chioroform
o-cresol
m-crcsol
__ p-cresol
cresol
1,4-dichlorobenzene ------1,2-dichloroethane
__ 1,1-dichloroethylene _____ _
2,4-dinitrotoluene
__ heptachlor
hexachlorobenzene
hexachlorobutadiene
hexachloroethane ------
__ methyl ethyl ketone _____ _
nitrobenzcne
__ pentaehlorophenol
__ pyridine
__ tetrachloroethylene
__ trichloroethylene
__ 2,4,5-trichlorophenol . ------__ 2,4,6-trichlorophenol _____ _
__ vinyl chloride
endrin
lindane
__ methoxychlor
__ tox3phene
2,4-D
_ 2,4,5-TP (Silvcx)
D N.C. Department of Environment,
I lcahh, & Nalural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box ~7, 306 N. Wilmington Street
Raleigh, North Carolina 27611
. 0., Number Neb D(; 2--sss 7C/ 2... Field Sample Number O( 7 2-'ob
. Name of Site St3rno/lS Stjzkc.. Site Location Sf cy-es //t //e.__.
g Collected By · J\ 'Z--ID# ___ Date Collected ~'20( 4'1 Time { 1L{5
m Agency: Hazardous Waste Solid Waste Vsuperfund
Sample Type
I Environmental Concentrate Comments
__ Ground water (1)
I __ Surface water (2)
I V Soil (3)
_· _ Other ( 4)
_ Solid (5) (MA 7>/+ -, I
_ Liquid (6) _ __,Q=---"6_" _____ _
-Sludge (7) _ ___.=::s~s_-_/c_:'3:::__·-;;;;Sc::cL ___ _
Other (8) ___________ _
Organic Chemistry
_ P&-:':GC/MS
Acid:E/N Ext.
MTBE
Results(mg/1)
Inorganic Chemistry
Parameter
-1:_ Arsenic
V Barium
v Cadmium
Chloride
Results~(mg/kg)
L. ::l
Jc:::_ Chromium
__ Copper
Fluoride
Iron
V Lead
v Manganese
VMercury
Nitrate
-<.. \ 0
3Q
lDO
v Selenium
----------------! V Silver .L..\Q
Radiochemistry
Parameter ~ Results (PCi/1)
__ Gross Alpha ______ _
Gross Beta
Microbiology
Parameter Results (Col/lOOml)
Sulfates
Zinc
pH
__ Conductivity
TDS
TOC
I Date Reccivcd _________ P.cportcd by _________ _
I D:ite Extracted. _______ Date Reeff ~145 AUG ZB 97
Date Analyzed_~------Lab Number _________ _
1)11<.; 1]!/1 (!/,..vis,·rt ?/(/1'\
TCLP Compounds
· foorganic Compounds
Arsenic
Barium
Cadmium,
Chromium
Lead
__ Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
p-cresol
cresol
1,4-dichlorobcnzene
1,2-dichloroethane
Results(mg/:)
Results(mg/1)
------
------
__ 1,1-dichloroethylene _____ _
2,4-dinitrotoluene
__ heptachlor .
hcxachlorobenzene
. hexachlorobutadiene ------hexachloroethane
• methyl ethyl ketone _____ _
nitrobenzenc
__ pentachlorophenol
__ pyridine
__ tetracn\oroethylene
__ trichloroethylene
__ 2,4,5-trichlorophenol _____ _
__ 2,4,6-trichlorophenol _____ _
__ ,inyl chloride
endrin
li1danc
methoxychlor
__ toxaphcne
_2,4-D
_ 2,4,5-TP (Silvex)
0, N.C. Department of Environment,
I lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State laboratory o{ Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
·•Dec Number A/C,L) Ct;; 2.-S"S5 71 L Field Sample Number _____ 6_(_7_Z:_9_7 ____ _
Name of Site SJ3rno/lS 'Se(11'c..-7Z:uilc.. Site Location _ _cS,._L_i:_/4.:i::c@--'='>'-'//:C-'1_/,_,hcoe....=----------
0 Collected By Ji f---ID# ___ Date Collected_Co~(='Z.=&,=· ::::(:::q=7====-.:T~im:e::._-=-=--/=SO-=-==S====-:...
o Agency: Hazardous Waste Solid Waste Vsuperfund
Sample Type
Environmental Concentrate Comments
__ Groundwater (1)
I __ Surface water (2)
I V Soil (3)
_ Other (4)
Solid (5)
-Liquid (6) __ _;:o;__~__,G"--11
_ _c_ ___ _
_ Sludge (7) _ _:_s_s_~_/ tJ.-'--1-_S_L ___ _
_ Other (8) __________ _
Organic Chemistry
_ P&T:GC/MS
Acid:13/N Ext.
MTBE
Results(mg/1)
Radiochemistry
Parameter Results (PCi/1)
__ Gross Alpha ______ _
Gross Beta
Microbiology
Parameter Results (Col/lOOml)
Inorganic Chemistry
Parameter
_Le_ Arser.ic
i_,,,-Barium
Result 4> 1"91 (mg/kg)
'-l
U Cadmium
Cl,Ioride
~-Chromium
__ Carper
Fluoride
Iron
V Lead
✓ Manganese
L/ Mercury
Nitrate
e,_ Selenium
L---Silver
. Sulfates
Zinc
_pH
5:-l
190
0. j 9
__ Conductivity ______ _
TDS
TOC
I Daie Received ________ Reported by _________ _
I
0;1lc Exlr;,iclcU Dc1lc Reporled -----01~~1-4-5~Au·-c~2~s9-7-
o,itc Analr1.cd Lab Number
TCLP Compounds
Inorganic Com pounds
Arsenic
Barium
Cadmium•
Chromium
Lead
__ Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-creSol
m-crcsol
__ p-cresol
cresol
Results(mg/1)
Results(mg/1)
------
1,4-dichlorobenzene _____ _
1,2-dichloroethane
1,1-dichloroethylene _____ _
2,4-dinitrotoluene
__ heptachlor
hexachlorobenzene
hexachlorobutadiene
hexachloroethane ------
__ methyl ethyl ketone _____ _
nitrobenzene
__ pentachlorophenol
__ pyridine
__ tetrachloroethylene
__ trichloroethylene
__ 2,4,5-trichlorophenol ----~-
__ 2,4,6-trichlorophenol _____ _
__ vinyl chloride
endrin
lindane
methoxychlor
toxaphene
2,4-D
2,4,5-TP (Silvex)
It N.C. Department of Environment, IJ I lcalth, & Natural Rcsourcc.s
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Labqratory of Public Health
P.O. Box 28047, 306 N. Wilmincton Street
Raleigh, North Carolina 27611
19'-Nu~ber NCO Gt;; z__ sS5 712... Field Sample Number 6 (]'Z <a%
Name of Site 5Jjrno/1 S '>t'fn'c..,. 7??,,11/c... Site Location Sfq./-es //1 //e_ D Collected By-"-"1------"""/\---=-z.....'--=~'-='---'ID-=#::~~~--Date Collected <i5{ z.s( q, Time ( q SC>
Hazardous Waste Solid Waste Vsuperfund
Sample Type
Environmental Concentrate Comments
__ Ground water (1)
I __ Surface water (2)
1 _ Soil (3)
.J[_ Solid (5) Siu~ /s.:,1'/
Liquid (6) \)e lovJ 1?fJ2c,!\ ii: 3
V Sludge (7) S S-c., i -/.)J .5
_ Other (4) Other (8)
Organic Chemistry
_ P&T:GC/MS
Acid:b/N Ext.
MTBE
Results(mg/1)
Radiochemistry
Pararnt:ter
__ Gross Alrha
Gross Beta
Results (PCi/1)
Microbiology .
Parameter Results (Col/lOOml)
Inorganic Chemistry
Parameter
<.--Arsenic
V Barium
vCadmium
Chloride
'-Chromium
__ Copper
Fluoride
Iron
Results..-:mg/kg)
'-l
V Lead v Manganese
v Mercury
--Nitrate
V Selenium
V Silver
Sulfates
Zinc
_pH
"'--10
""-\ 0
310
<IQ
__ Conductivity ______ _
TDS
TOC
I Dale Received ________ Reported by _________ _
Dale Extrncled Dal C Rel'{)red ._____ . v. ~147 AUC 2897 I . Dale Analy1.ed Lab Number ~=----------------f}j]S .1l'JI (l{cvi.scd 2/91)
TCLP Compounds
l.10rga1,ic Compounds
Arsenic
Barium
Cadmium,
Chromium
Lead
__ Mercury
Selenium
Silver
Organic Compounds
benzene
carbor, tetrachloride
chlordane
chlorobenzcne
chloroform
o-cresol
m-cresol
__ p-cresol
crcsol
1,4-dichlorobenzene
1,2-dichloroethane'
Results(mg/1)
Results(mg/1)
------
------
__ 1,1-dichloroethylene ______ _
2,4-dinitrotoluene
__ heplachlor
hexachlorobenzene
hexachlorobutadiene
hexachloroethane
__ methyl ethyl ketone
nitrobcnzene
__ pentachlorophenol
__ pyridine
__ tetrachloroethylene
__ trichloroethylene
-------
-------
__ · 2,4,5-trichlorophenol _____ _
__ 2,4,6-trich.lorophenol _____ _
__ vinyl chloride
endrin
\indane
__ methoxychlor
__ toxaphene
2,4-D
_ 2,4,5-TP (Silvex)
I , N.C. Dcpunmcnt of Environment,
1 !c.allh, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
sss 712... Field Sample Number
S1atc Laboratory of Public Health
P.O. Box 2W7, 3J6 N. Wilmington Street
Raleig.h, North. Carolina 27611
0(7-z_'3C · l)ee Number Alco Ct;; z_
S1d-esVr lie.-Name of Site C./ r Yf n'e,_ ]q_/l/c. Site Location -:3mot1S
D Collected By µ/JJ ID# Date Collected 0{z1.p(qJ Time oq£o
D Agency: Hazardous Waste Solid Waste Vs uperfund TCLP Compounds
--
Sample Type -Inorganic Compounds Results(mg/1)
m Environmental Concentrate Comments Arsenic --
S (ucb e /soi I Barium --
__ Groundwater (1) VSolid (5) Cadmium, --
I #-S Chromium
pelow /~jDU\ --
__ Surface water (2) _ Liquid (6) Lead --Mercury
I _ Soil (3) V Sludge (7) ss-7-7--Gu.S --Selenium --Silver --
Other ( 4) _ Other (8) --
I --
--
Organic Chemistry Inorganic Chemistry --
I P1:1rametcr Results(mg/1) Parameter Results...a (mg/kg) Organic Compounds Results(mg/1)
_P&T:GC/MS V Arsenic ..( "l benz:ne --
Acid:B/N Ext. V Barium 'C--0 carbon letrcchloride --
MTBE v Cadmium .t_ l Cl chlordane ------
Chloride chlorobenzene ------v Chromium ~ chloroform ----
I --Copper o-crcsol ----
--Fluoride m-cresol ----
--Iron __ p-cresol --
I --v Lead l +. ere.sol
17" ').So --
--Manganese --1,4-dichlorobenzene
--v-Mercury L._ c,_ \ 1,2-dichloroethane
--Nitrate · __ 1,1-dichloroelhylene
I --
V Selenium ~ .;i 2,4-dinitrotoluene --
V Silver L.. ·1 Cl __ heptachlor --
Radiochemistry Sulfates hexachlorobenzene
I ----
······-·· Zinc . hexachlorobutadienc
Parameter ----
Results (PCi/1) _pH hexachloroethane --
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Beta TDS nitrobenzcne ----TOC __ pentachlorophenol --
--__ pyridine
I Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophenol
------vinyl chlodde
endrin --
I
lindane
Date Received
--
Reported by __ methoxychlor
__ toxaphenc
Dole ExlraclcJ Date Rer61e~ : 2,4-0
I
--148 AOC 2897 _ 2,4,5-TP (Silvcx)
[_)<.tic Ana!y1.cd Lab Number --
IHII..: 1Hl1 fllr,·;~,.,1 ")/(Jl)
0 N.C. Department of Environment,
\lcalth, & Natural Resources
Solid Waste Management Division
SAM.PLE ANALYSIS REQUEST State Laboratvry of Public Health
P.O. Box 28047, 306 N. Wilrr.ington Street
Raleigh, North Carolina 27611
. lie: Number AfC.Q {>r;; 2-S-SS 7C/ Z... Field Sample N:;mber 0(7210
Name of Site S(jrno/1.5 Sq?n'c_ 7?<./1./c.. Site Location Sfql-cy VI l le....
g Collected By-"4-~'-S=-=-f::-~=-'-'=--~lc.:Dc,#~~~---_ Dale Collected Q,/74 ( 17 Tim~ L Cf:(--z.._
I Agency: Hazardous Waste Solid Waste Vsuperfund
I
Sample Type
Environmental Concentrate Comments
__ Ground waler (1)
I __ Surface water (2)
VSolid (5) Sf ucfje..
1
p1/e..
q 1, -1 r) tr _ Liquid (6) __ _,____ _ _,_v _____ _
, _ Soil (3)
Other (4)
VS!udge (7) __ s_ .. _S_-_?-_3_-_w_.s __ _
Other (8)
I
Organic Chemistry Inorganic Chemistry
P&T:GC/MS
Acid:B/N Ext.
.. MTBE
Results(mg/1) Parameter
-1,::___ Arsenic
1..--Barium
I/ Cadmium
Chloride
V Chromium
__ Copper
Fluoride
Iron
v Lead
Result"' .1.(,ug/kg)
3. "1
L..."'\.S:
190
11,,,0
v Manganese
V Mercury
\ '-\ D
0,39
Nitrate
c... Selenium
----------------l v Silver \ '-l
Radiochemistry
I Parani"eler Results (PCi/1)
Sulfates
Zinc
_pH
__ Gross Alpha ______ _
Gross Beta
I Microbiology
1------1
Parameter Results (Col/lOOml)
__ Conductivity
TDS
TOC
I Date Received ________ Reported by _________ _
D:itc Extractc<l Date RepS'{lf<}-, 1,. ...
I -----u1..:: -~9 AUC 2697
Date An:ilyzed Lab Number
l)l!S 31'}! {il,cvisc~d72~/9~1,----------------
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium.
Chromium
Lead
__ Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
ehlorobenzene
chloroform
o-cresol
m-cresol
__ p-cresol
cresol
1,4-dichlorobenzene
1,2-dichlorocthane
Results(mg/1)
Results(mg/1)
------
1,1-dichloroethylene _____ _
__ 2,4-dir.itrololuene
__ heptachlor
hexachlorobenzene
hexachlorobutadienc ------hexachloroethane
__ methyl ethyl ketone _____ _
nitrobenzcne
_· _ pcntaehlorophenol
__ pyridine
__ lelrachloroethylcne
__ trichlcroethylene
2,4,5-trichlorophenol _____ _ = 2,4,6-triehlorophenol
__ vinyl chloride
endrin
lindane
melhoxychlor
tor.aphene
2,4-D.
_· 2,4,5-TP (Silvcx)
D'N.C. Department of Environment,
I lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Rox 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611.
(9: Number Alco {)(; Z-sS5 712... Field Sample Number 0(72. Cz (
Name of Site_S/_g,_,'q;.m'--"'o"--/1:..;:S=:.
1 ~Yf==,cc-/i_:_'..::c_::..__-1.74__,::o.'-'/l"-/c_---'---Site Location Sfd-eJ V! '( /e__ 0 Collected By ____ f_'l _1.--____ ID# ___ Date Collected 0{-z.e,, ( q 1 Time __ /~(~/~11 __
m Agency: Hazardous Waste Solid Waste Vsuperfund
Sample Type
Environmental Concentrate Comments
__ Ground water (1)
I __ Surface water (2)
1 _ Soil (3)
Vsolid (5) S{ uJ~,e_ 2; (e_ J (
_ Liquid (6) -----"be=-ce+e...:...Tt.__:__-=·2-=---·'--F+"----_ I
~Sludge (7) __ S_.S_-_-Z_4_-_LU_~ __ _
_ Other (4) _ Other (8)
Organic Chemistry Inorganic Chemistry
Results(mg/1) Parameter
_k:.Arsenic
V Barium
ResuH'tt ,ICJl(~g/kg)
_ P&T:GC/MS
Acid: B /N Ext.
MTBE -----v Cadmium
Chloride
t.---Chromium
__ Copper
--Fluoride
Iron
V .Lead
V Manganese .
7:T Mercury
Nitrate
-r;-selenium
----------------! V Silver
Radiochemistry
Paramder Results (PCi/1)
__ Gross Alpha· ______ _
Gross Beta
Microbiology
Parameter Results (Col/lOOml)
Sulfates
· Zinc
pH
__ Conductivity
-TDS
TOC
_3_9
?,qo
I Dale Received ________ Reported by _________ _
Dale Extracted Dale Reported ·
I ._____ 012150 A0G2697
Date· Analyzed Lab Number
1)11<.; 1\IJI (nrvi\1•d //91'\ ----------
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium.
Chromium
Lead
__ Mercury
Selenium --Silver
Organic Compounds
benzene
carbon tetrachloride
ch,ordane
chlorobenzene
chloroform
o-cresol
m-cresol
__ p-cresol
cresol
1,4-dichlofobenzene
1,2-dichloroethane
Results(mg/1)
Results(mg/1)
------
__ 1,1-dichloroethylene _____ _
_-_-2,4-dinitrotoluene
heptachlor
hexachlorobenzene
hexachlorobutadiene
hexaehloroethane
__ methyl ethyl ketone
nitrobenzcne
__ pentaehlorophenol
__ pyridine
__ tetrachloroethylene
__ trichloroelhylene
__ 2,4,5-trichlorophenol
__ 2,4,6-triehlorophenol
vinyl chloride
endrin
bdane
__ methoxychlor
toxaphene
-2,4-b.
2,4,5-TP (Silvcx)
------
------
------
IJ N.C. Ocpanmcnt of Environment, IJ I lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box: 28047, 3G6 N. Wilmington S:rect
Raleigh, North Carolina 27611
lite Number /V'C.,Q C(; Z-SS5 7C/ Z... Field Sample Number ____ 0_/_7_2:_1_· _?,, _____ _
• Name of Site SJ3rno//S sq:,·kc:,,, ']a./l/c. Site Location. _ __,S-,;cf,Jey:..:::..=,::._V_,_1_,_/_,_/e_=---------u Collected By--'-"lc.:...:.,=-'-"/1:...,' -'L-=~,:__:::c___.I._,D"'#~:~~---_ Date Collected __ 0---=--'-(_rz,_(p----'-(.-'q_7~--Time _ _.,,/_0-"5_,_Cj' __
I Agency: Hazardous Waste. Solid Waste Vsuperfund
Sample Type
Environmental Concentrate Comments
Vsolid (5) · __ Groundwater (1)
I __ Surface water (2) _ Liquid (6) _b_e.~_,_,\~_3_-Fe_e_t--/--'----_
u
, _ Soil (3)
Other ( 4)
V Sludge (7) __ S_S_-_~_s_-_w_.s __ _
Other (8) ___________ _
Organic Chemistry Inorganic Chemistry
Results(mg/1) Parameter Results~(mg/kg)
P&T:GC/MS
Acid:B/N Ext.
MTBE
Radiochemistry
P..irameter Results (PCi/1)
__ Gross Alpha ______ _
Gross Beta
Microbiology
Results (Col/lOOml)
L,,-Arsenic ""-3 _ 9
V Barium
v Cadmium < 9 _ R
Chloride
L--Chromium
Copper
Fluoride
Iron
t.., Lead
v Manganese
V Mercury
Nitrate
V Selenium
V Silver
Sulfates
Zinc
_pH
__ Conductivity
TDS
TOC
3:':\0
•.. Date Receivcc _________ Rcportcd by _________ _
Date Extractc<l Date R;jlorted
I ----u121-~1~Am□-cz=5-97-
oatc Analy-,cd Lab Number
"11<.: 11111 r11,,,.;, . ..,1,l(n'\ ----------
TCLP Compounds
Inorganic Compounds
Arsenic
Ba:ium
Cadmium,
Chromium
Lead
Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
rn-cresol
__ p-eresol
cresol
1,4-dichlorobenzene
--1,2-dichloroethane
Results(mg/1)
Results(mg/1)
------
------
__ 1,1-dichloroethylene _____ _
2,4-dinitrotoluene
__ heptachl0r .
hexachlorobenzene
. hexachlorobutadicne
hexachlorocthane ·
methyl ethyl ketone
ni!robenzene
__ pentachlorophenol
__ pyridine
__ tetrachloroethylene
__ trichloroethylene
------
__ 2,4,5-trichlorophenol _____ _
__ 2,4,G-trichlorophenol _____ _
__ vinyl chloride
endrin
liadane
methoxychlor
toxaphene
2,4-0
_ 2,4,5-TP (Silvex)
I, ·N.C. Ocpanmcnt of Environment,
I 1c::)1h, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
-le, Number...:.AA__.:_C,=Q'-0(;=-><c..::Z....=--.c::S"_S___:5=-----=7_1,.__Z.. ___ Field Sample Number O( 7 z__q f
Name of Site SJ3mo/l .S '5t'f-fi 'c... ]4;1 /c.. Site Location Sf q)--ey {// '( /e___
I Collected By-'-"1------'-"-'-'--"'--b=--z__..=r-~~J~D~#==~~~ Date Collected Co{zJ; (q1 Time / O sr
I Agency: Hazardous Waste Solid Waste Vsuperfund
I
Sample Type
Environmental Concentrate Comments
__ Groundwater (1)
I __ Surface water (2)
V Solid (5) -_s=· _/u_c_/J+e,--,('-Y_I/_£-__
-Liquid (6) _1"/)_;:.......,..,f_l_i'C=-?_-ft_--l-(-----'3_ti__.:_--f_._
v Sludge (7) __ s_s_-_c.1_-2.c_s_-_W_J:: __ I_ Soil (3)
_ Other (4) _ Other (8) ___________ _
Organic Chemistry Inorganic Chemistry
_P&:T:GC/MS
Acid:B/N Ext.
MTBE
Results(mg/1) Parameter
v Arsenic
l,---Barium
Result"4 g¢'P(rog/kg)
<'.'... 3_9
L-Cadmium
Chloride
v Chromium
__ Copper
Fluoride
Iron
JL... Lead
~ Manganese
_£ Mercury
Nitrate -
V Selenium
---------------l V Silver
Radiochemistry
Gross Alpha
Gross Beta
Results (PCi/1)
Microbiology
Results (Col/lOOml)
Sulfates
Zinc
pH
__ Conductivity
TDS
TOC
300
'70
I Date Received ________ Reported by _________ _
Date Extracted Date Rep('ff~iSz AUG 28 97 I Date Analy"l.ed ________ LaiJ Number
1)1!<.; 11!!1lllr,,;,.,,,11/()J\ ----------
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium•
Chrnmium
Lead
Mercury
--Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
__ p-cresol
cresol
1,4-dichlorobenzene
1,2-dichloroethane
Results(mg/1)
Results(mg/1)
------
------
__ 1,1-dichloroethylene _____ _
2,4-dinitrotoluene
__ heptachlor
hexachlorobenzene
. hexachlorobutadiene
hexachloroethane
__ methyl ethyl ketone
nitrobenzene
pcntachloroph~nol
--pyridine ·
__ tetrachloroethylene
__ trichloroethylene
__ -2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol
__ vinyl chloride
endrin
lindane
methoxychlor
.. toxaphcne
-2,4-0 -
_ 2,4,5-TP (Silvex)
------
I' N.C. Department of Environment,
I lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
sss 7C/Z... Field Sample Number
State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
6(7ZC/-f lie: Number NCO C\'o Z..
Sf des VI l I e_ Name of Site SJ3rno// 's St:(·kc 7"a.;1/c. Site Location
I Collected By A -z_ ID# Date Collected ea{_zf,, I q') Time UM
I Agency: Hazardous Waste Solid Waste Vsuperfund
I
I
I
Sample Type
Environmental
__ Ground water (1)
__ Surface water (2)
V Soil (3)
_ Other (4)
Concentrate
_·_ Solid (5)
_ Liquid (6)
_ Sludge (7)
_ Other (8)
Comments
s-nr '.1j? ~ /\. I:-<; C 10":>)
S S-7,.&,-Sl
Organic Chemistry Inorganic Chemistry
P&T:GC/MS
Acid:B/N Ext.
MTBE
Results(mg/1) Parameter
(..,,-' Arsenic
-C:Barium
v Cadmium
.----Chloride
v Chromium
__ Copper
Fluoride
Iron
Results.--(mg/kg)
-<-3.9
l.J.o
so
I=---/..., Lead
l/" Manganese
(,,-Mercury <0.10
Nitrate I L----Selenium
r---------------l l/Silver
Radiochemistry.
I Parameter
__ · Gross Alpha
Gross Beta
Results (PCi/1)
Microbiology
Parameter Results (Coi/lOOml)
Sulfates
Zinc
_pH
_·_ Conductivity
TDS
TOC
I Date Receivcd ________ Rcported by _________ _
Dc,tc Extracted Dale Rep'f'it.ar ------vi.'2153 AUG 2697 I Dale Analy1.cd Lab Number
1)11'-1,)1)1 11:,.,.,~,·ri J/(/1' ----------
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium,
Chromium
Lead
__ Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
__ p-cresol
cresol
1,4-dichlorobenzene
--1,2-dichlorocthane
Results(mg/1)
Results(mg/1)
------
------
__ 1,1-dichloroethylene _____ _
__ 2,4-dinitrotoluene
._ .. _ heptachlor
hexachlorobenzene
hexachlorobutadiene
hexachloroethane
__ methyl ethyl ketone
nitrobenzene
------
__ pentachlorophenol . _____ _
__ pyridine
__ tetrachloroethylene
__ trichloroethylene
__ 2,4,5-trichlorophenol _ _;_ ___ _
__ 2,4,6-trichlorophenol
__ vinyl chloride
·endrin
lindane
__ methoxychlor
toxaphcnc
2,4-D
_ 2,4,5-TP (Silvex)
I. N.C. Depanment of Environment,
I lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
~ Number NCO 00 Z-SS5 71 Z.... Field Sample Number 0/7 2, '9 S
Name of Site S(_jrno/1 S 4·kc__ 7a,/l/C.. Site Location Sfd-er n //e.. I Collected By'-.L>!J,:.;,.,:,,e:...:..s:::~~==-c-=-1'-'D"'#~:~~~-Date Collected 0c(z<r ( C/1 Time {If{,
I Agency: Hazardous Waste Solid Waste Vsuperfund
Sample Type
Environmental Concentrate Comments I
__ Groundwater (1)
I __ Surface water (2)
I V Soil (3)
_ Solid (5) S,.._,,,~ce S.Dt /
_ Liquid (6) __,0"""--'4J'-''c;"'"c.:..:ecc.r--_+-_-tl)-'-'-___ _
_ Sludge (7) _"'5=-cc;\-tr_O+&'t---~~· __ ±4_· ~-
_ Other (4) -Other (8) __ S___cc.S_-_7.c...";-'----'S,=-L_· __ _
Organic Chemistry Inorganic Chemistry
Results(mg/1) Parameter Results~mg/kg)
P&T:GC/MS L,,.--Arsenic L;. 3,9
Acid:B/N Ext. V Barium d.0
MTBE l.,--Cadmium ,e:_9_3
Chloride
(.,. Chromium :::i _;;,_
__ Copper
Fluoride
Iron
_LLead <C..9.2.
L--Manganese (o ?',
L.,-Mercury < Q, t.o
Nitrate
v-Selenium .L. '.J-.
7:7 Silver L9.R
Radiochemistry Sulfates
Zinc
Parameter Results (PCi/1) _pH
__ Gross Alpha __ Conductivity
Gross Beta TDS
TOC
Microbiology
Results (Col/lOOml)
I Date Received Reported by
D:itc Exlraclc<l Dale RqO1e~ I 154 AUG 2e97
Dale Analy1,cd Lab Number
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium,
Chromium
Lead
__ Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
rn-cresol •
__ p-cresol
cresol
1,4-dichlorobenzeoe
__ 1,2-dichloroethane
__ 1,1-dichloroethylene
2,4-dinitrotoluene
__ heptachlor
hexachlorobenzene
. hexachlorobutadiene
hexachloroethane
__ methyl ethyl ketone
nitrobenzene
__ pentachlorophenol
__ pyridine
__ tetrachloroethylene
__ trichloroethyleoe
__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol
__ vinyl chloride
endrin
!indane
__ methoxychlor
__ toxaphcnc
2,4-D
_ 2,4,5-TP (Silvex)
Results(mg/1)
Results(mg/1)
0, N.C. Department of Environment,
I \calth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Strec!
Raleigh, North Carolina 27611
gee Number Alco Gt;; 2.-sss 71 z... Field Sample Number ___ _::0/::.._7-'--Z_'f,;__C:: ______ _
. Name of Site S(jrno/1 s sq::rkc... ?a,/1./c.. Site Location_--'S'"""-t'-'qjey'-'-'""--'~C-'/C..',_/'-"/e__=----------
g Collected By Sk--ID# ___ Date Collected. __
0
_ey_c_1._1o_·_,_(--'q-7'-----Time_(;;_7..._o_:s::.._ __
g Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds
----
Sample Type Inorganic Compounds Results(mg/1)
g Environmental Concentrate Comments Arsenic --
bow!\ Dc,,.J/t,d-cI'-Barium --Cadmium, __ Groundwater (1) Solid (5) --g Chromium
~0ff-, ~Jc~ --
__ Surface water (2) _ Liquid (6) Lead --
be,pd0 ?:,-~l(z, ~f-
__ Mercury
g VSoil (3) _ Sludge (T) Selenium --Silver
SS-2 ~-S,L --
_ Other (4) _ Other (8) --
E
--
--
Organic Chemistry Inorganic Chemistry --
E Parameter Results(mg/1) Parameter Results~ (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS (,,-Arsenic 3.9 benzene ----
Acid: B /N Ext. (., Barium 'lS carbon tetrachloride --
MTBE 1..--Cadmium <9.8 chlordane ----
Chloride chlorobenzene ------
L---Chromium ..110 chloroform ----n --__ Copper o-cresol --
--Fluoride m-cresol ----
--Iron __ p-cresol --
D --(..,,-Lead <9.8 cresol --
--_.s:._ Manganese \50 --1,4-dichlorobenzene
--i'.:_ Mercury -<0.,1..0 --1,2-dichloroethane
n ----Nitrate 1,1-dichloroethylene --
G-Selenium L.,.:;).._ 2,4-dinitrotoluene
<9_6 --
V Silver heptachlor --
D
Radiochemistry Sulfates hexach loroben,,ene ----
''"'•-·· Zinc hexachlorobutadiene
Parameter ----
Results (PCi/1) _pH hexachloroethane --
u
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
--Gross Beta TDS nitrobenz.ene --TOC __ pentachlorophenol --
--__ pyridine
u Microbiology --__ tetrachioroethylene
--__ trichloroethylene
Parameter Results (Col/l00ml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --
g lindane
Date Received
--
Reported by . __ methoxychlor
__ toxaphene
Dale Extractcu Date Reported 2,4-D
m 012155 ADC 2897 --_ 2,4,5-TP (Silvcx)
Dale Analyzed Lab Number --"' ,, . ., "" '" . .,,.,,,
I N.C. Dcpa11mcnt of Environment,
I !cahh, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
le, Number NCO Q;; Z. SS5 7C/ Z... Field Sample Numbe: O( 7 -Z., 77
Name of Site S(gmo/1.S 5etn'c_. 7z:ui./c.. Site Location Sfqjey Vil /e_
I Collected By-~;_;_;_:"'--'-=s:..._l-~=F''----'--=-----'I'--'D"'#~~~~---_ Date Collected 'c/zs. / 4'7 Time (:Y7
I Agency: Hazardous Waste Solid Waste Vsuperfund
Sample Type
Environmental Concentrate Comments
Solid (5) --. __ Ground water (1)
g __ Surface water (2)
D V Soil (3)
-z I( --? { '0-:'-Li _ Liquid (6) ______ v _ _,~ __ c_ "'-_
Sludge (7) __ ss __ -_-z~q_-_S_L __ _
_ Other (4) _ Other (8) ·-----------
Organic Chemistry Inorganic Chemistry
P&T:GC/MS
Acid:B/N Ext.
MTBE
Results(mg/1) Parameter
L-Arsenic
TBarium
v Cadmium
Chloride
Resul'-♦ WI°' \mg/kg)
-3 -c,
_L Chromium
Copper
Fluoride
Iron
v Lead
L--Manganese
L----Mercury
Nitrate
le::__ Selenium
----------------l /,,-Silver
Radiochemistry
Results (PCi/1)
Gross Alpha -------Gross Beta
Microbiology
Results (Col/lOOml)
Sulfates
Zinc
pH
Conductivity
TDS
TOC
;;,,a
i(J
I Date Received ________ Reported by _________ _
D:ilc ExlractcJ Dale Reported
I ----O12-1s-6~Au-c2~0-97~
Dale Analyzed Lab Number ~~----------------
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium·
Chromium
Lead
__ Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzcne
chloroform
o-cresol
m-cresol
__ p-cresol
cresol
1,4-dichlorobenzene
--1,2-dichlorocthane
Results(mg/1)
Results(mg/1)
------
------
__ 1,1-dichloroethylene _____ _
2,4-dinitrotoluene
__ heptachlor
hexach lorobenzene
hexachlorobutadiene
hexachloroethane ·
__ methyl ethyl ketone
nitrobenzcne
__ pentachlorophenol
__ pyridine
__ tetrachloroethylene
__ trichloroethylene
__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol
__ vinyl chloride
endrin
lindane
__ methoxychlor
toxaphenc
2,4-0
__ 2,4,5-TP (Silvcx)
------
IN.C. Department of Environment,
1 lcalth, & Nalural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory o{ Public Health
P.O. Box 28047, 306 N. Wilmington Street
RB!eig.h, North Carolina 27611
.. Number Alco 0?:i z__ sss 71 z_ Field Sample Number 017 2-'fg
Name of Site SJ3rno/l S St:fkc__ 7a,;i/c. Site Location :S1q./--es (/( //e.....
I Collected By--'--"1-~s""· -'-f::__"'---=CF----=~-'I'-'D"'#::~~~-Date Collected 0/ U I 11 Time r 3 3 7
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds
----
Sample Type Inorganic Compounds Results(mg/1)
0 Environmental · Concentrate Comments Arsenic --
f3ac~I'?( S'Or '(
Barium --
__ Groundwater (1) Solid (5) Cadmium· --
D Chromium
j lh,_ ~4-I t}e,( fP'\ --
__ Surface water (2) _ Liquid (6) Lead --
SS-:::o ~S/_..
__ Mercury I V Soil (3)_ _ Sludge (7) Selenium --Silver --
_ Other (4) _ Other (8) --
I --
--
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results...-i (mg/kg) Organic Compounds Results (mg/I)
P&T:GC/MS /_,Arsenic .5_ 9 benzene --
Acid:13/N Ext. V Barium < ,;;J.Q carbon tetrachloride --
MTBE L---Cadmium <'...9 .R chlordane ------
Chloride chlorobenzene ------
v-Chromium 1DCI chloroform ----
I --__ Copper o-cresol --
Fluoride m-crcsol ------
--Iron __ p-cresol --
I --· v-Lead 1 i cresol
L--Manganese
--
--\ 'l D --1,4-dichlorobcnzene
--v Mercury (Q,[C;_ 1,2-dichloroethane
I --Nitrate __ 1,1-dichloroethylene --v Selenium L;)... 2, 4-dinitrotoluene ----
l--Silver <9.A __ heptachlor --
I
Radiochemistry Sulfates hexachlorobenzene ----
······-·· Zinc · hexachlorobutadiene
Parameter ----
Results (PCi/1) _pH hexachlorocthane --
I
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol --
--__ pyridine
I Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
'-= --__ 2,4,6-trichJorophcnol
--_· _ vinyl chloride
endrin --
I lindane
Date Received
--
Reported by . methoxychlor --
--toxaphcne
Dale ExtracleJ Dale Rcp0tcd 2,4-0
I 121'.l't' AUG 2897 --_ 2,4,5-TP (Silvcx)
Dale Analyzed Lab Number --""•· "'"" ,,,_ . . ... ,, " '
I N.C. Department of Environment,
I lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
le-, Number Ale)) Or;; 2-sss 71 z... Field Sample Number .. 0/7 zqa
Name of Site S(3mo/l .S S;pn'c... 7a,/!/c. Site Location Sfq..iey Vil /e_ I Collected By-"'-"/--'-'C:.CS...:..=/c'--=CF'--='----'1--=D#~:~~~~ Date Colleded 0o(z..<:;,.( 11 Time_---'--/4{_,_,_.:=o __
I Agency: Hazardous Waste Solid Waste Vsuperfund
I
Sample Type
Environmental Concentrate Comments
__ Ground water (1)
I __ Surface water (2)
I \/soil (3)
-_ Other (4) ·
_ Solid (5) f?::a_~ 2>bl' /
_ Liquid (6) --'-1-'--Z_-_tt-'---_-_d--i.ef'-"tb...'---_
-Sludge (7) _ __::s:::_s_-_;:,=c_l _~_<;._L __ _
_O~rOO __________ _
Organic Chemistry
_P&T:GC/MS
Acid:B/N Ext.
MTBE
Results(mg/1)
Radiochemistry
Parameter
__ Gross Alpha
Gross Beta
Results (PCi/1)
Microbiology
Parameter Results (Col/lOOml)
Inorganic Chemistry
Parameter
l-Arsenic
t..,,..-Barium
V Cadmium
Results---(mg/kg)_
L_ .3_ 9
Chloride
_L_ Chromium
__ Copper
Fluoride
Iron
_lL Lead
__1::_ Manganese
v Mercury
--Nitrate
v Selenium
<----Silver
Sulfates
Zinc
_pH
__ Conductivity
TDS
TOC
dD
5DQ < o,IO
.L....J--
I · Date Received _________ Reported by _________ _
Date Extracted Dale Reported
I -----O12~1~5~8~Am0=cz=5~9~7-
oate Analy1.ed Lah Number
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium·
Chromium
Lead
__ Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
__ p-cresol
cresol
1,4-dichlorobenzene
1,2-dichloroethane
Results(mg/1)
Results(mg/1)
------
------
__ 1,1-dichloroethylene _____ _
2,4-dinitrololuene
__ heptachlor
hexachlorobenzene
hexachlorobutadiene
hex a ch lo roe thane ---'----
__ methyl ethyl ketone _____ _
nitrobenzcne
_-_ pentachlorophenol
__ pyridine
__ tetrachloroethylene
__ trichloroethylene
__ 2,4,5-trichlorophenol _____ _
__ 2,4,6-trichlorophenol _____ _
__ vinyl chloride
endrin
lindane
__ methoxychlor
__ toxaphene
2,4-D
2,4,5-TP (Silvex)
I N.C. Depat1mcnt of Environment,
\ lcalth, & Natural Resources
Solid Waslc Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Oox 28047, 306 N. Wilming10n StrcCt
Raleigh, North Carolina 27611
119c Number Alco Or:;; z.__ sS5 71 z... Field Sample Number (!)(7 300
Name of Site S(jrno/1 S Stf-kc... 7?!,/l/c... Site Location Sfqfey VI //e_.
I Collected By--"-"l'--'-'-'"'j--'5=-~=1':.C..:..=---'ID--=#::~~---_ Date Collected ca(zs. (en Time_,_/....:'o:c:.__'2.'_S:. __ _
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds
----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
"'::e d 1' rn e {\ + Barium --
__ Ground water (1) _ Solid (5) Cadmium• --
I __ Surface water (2) Be/a0 H-'V\~rl:tA
Chromium --
_ Liquid (6) Lead --
~d __ Mercury I V Soil (3) _._. Sludge (7) Selenium
I --Silver
SS-l I G -s IJ --
_ Other (4) _ Other (8) --
I --
--
Organic Chemistry Inorganic Chemistry --
~ Parameter Results(mg/1) Parameter Resul!s (JSffllJ' '.;ng/kg) Organic Compounds Results(mg/1)
_P&T:GC/MS v-Arsenic 4-. .3 -"°I benzene --
Acid:B/N Ext. L---Barium .].,[) carbon tetrachloride --
MTBE .J.L__ Cadmium .,,., 9 ... -2 chlordane ----
Chloride chlorobenzene ------v Chromium 'f 1-} chloroform ----
~ --__ Copper o-cresol --
--Fluoride m-cresol ----
--Iron p-cresol --
~ --L---Lead ~9_g cresol
L--Manganese --
--<.,_3 --1,4-dichlorobenzene
--J.L Mercury <o.{Q --1,2-dichloroethane
~ --Nitrate __ 1,1-dichloroethylene
C--Selenium ~2, 2,4-dinitrotoluene
1L._ Silver -<. 'j_ R __ heptachlor
E
Radiochemistry Sulfates hexachlorobenzene ----
······-·· Zinc . hexachlorobutadiene
Parameter ----
Results (PCi/1) _pH hexachloroethane --
__ Gross Alpha __ Conductivity --methyl ethyl ketone
~ Gross Beta TDS ·-nitrobenzene ----TOC __ pentachlorophenol --
--__ pyridine
I Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
I.----__ 2,4,6-trichlorophenol
--__ vinyl chloride
endrin --
I
lindane
Date Received
--
Reported by --methoxychlor
-· toxaphcne --
Dote ExtroctcJ Osle Re0rled 697 2,4-D --121)9 ~UC Z _ 2,4,5-TP (Silvex)
Dole Analyzed Lab Number I --1\1 t~• -,,.,,In-.. : .. _,,-, 11'1\
• N.C. Ocp.inmcnt o{ Environment, I 1 lcal!h, & Nalura\ Rcs.ourccs
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Hca\\h
P.O. Box 280-47, 306 N. Wilmington Street
Raleigh, North Carolina 27611
•• e Number NCO l;(, z.... ss.s 71 z.. Field Sample Number CD I 7~o
· Name of Sile S,t;mo//c'.s $q::-kc:__ 7?<,;1/c.. Site Location Sfcy-esvr //e__
I Collected By ._.r 6 --z._ JD# ___ Date Collected ca/v{ 1'1 Time (7 s. 3
I Agency: Hazardou.s Waste Solid Waste Vsuperfund TCLP Compounds
----
Sample Type Inorganic_ Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
JO-iV\ c'. .:S
Barium
V Ground water (1) wfl I --
_Solid (5) --Cadmium,
I
Chromium
ss-u2.--Ft-u --
__ Surface water (2) _ Liquid (6) Lead --
D l<-i N \L-1 t\/ 4-WA ,ER-U.C-Q._ --Mercury
_ Soil (3) _ Sludge (1) Selenium
I -----Silver
_ Other (4) j(_f\Gt.-'!\ Lt, "'-izi ,.,,_,, /Vtl'f,\_ --
Other (8) --
I --
--
Organic Chemistry Inorganic Chemistry --
u Pnrameter Results(mg/1) Parameter Results(mg/1) •mif ;i Organic Compounds Results(mg/1)
_ P&T:GC/MS v Arsenic <o. O( benzene --
Acid:B/N Ext. V Barium /J ~ carbon tetrachloride
MTBE V Cadmium
--<✓;,oC chlordane ------
Chloride chlorobenzene
----<o. ol --v Chromium chloroform --
m --Copper o-cresol ----
--Fluoride m-cresol ----
--Iron p-cresol
( t.J, /JO,~
--
I --...lL:_ Lead crcsol --
--L/ Manganese (2_, 1,,S---1,4-dichlorobenzene
--V Mercury D. C.C\':) 1,2-dichloroethane --
I --(/ Nitrate 1, 1-dichloroethylene ----
V Selenium .L..Q-~\ 2, 4-dini troto luene
•.. --
[/ Silver <Q, < --heptachlor
.. . -Radiochemistry Sulfates hexachlorobenzene
I ----
'"•··-·· Zinc hexachlorobutadiene
... Parnrnetcr Results (PCi/1) ----
"7 JW.-hexachloroethane
__ Gross Alpha --Conductivity __ methyl ethyl ketone
I Gross Beta TDS nitrobenzene
------
TOC pentachlorophenol ----
----pyridine
I Microbiology ----tetrachloroethylene
__ trichloroethylene --
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
'" --__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --
I
lindane
Dote Received
--
Reported by methoxychlor --
--toxaphc!~e
I D~llc Exlrac((;J Date Reported 2,4-D
012113 ADC i:'.8 97 _ 2,4,5-TP (Silvcx)
Dale Aniilyctd Lah Number -
"' ... -.. , .. . -,,
I i'-'.C. Department of Environment,
1 lcallh, & Nalural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Oox 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
.. e Number NCO ~ Z.... SS5 7C/ 2... Field Sample Number ____ 0_/'_1'2 __ u._;,..,_{ _____ _
Name of s,ic St3rno/l S 5qzkc 7?<,;1,/c.. Site Location _ _,S....c:.fq.f-es;___:_-=..:..//..,_1..,_/.1-/e_=---------
1 Collected By "x:'-JD# Date Collected g( 7...J( 17 Time //I L. ---------~-----------'----
I Agency: Hazardous Waste Solid Waste VS u per fund TCLP Compounds
----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
'.:ll"pp-erJ UJel/
Barium
V Ground water (1)
--Cadmium _Solid (5) --
I Chromium
b(L,J /J i:-i NCr e,vl'\'ftlt, l)JE(L. --
_· _ Surface water (2) _ Liquid (6) Lead --
Sr-0 ?:,-Ft:,u --Mercury
I _ Soil (3) _ Sludge (7) Selenium --Silver
k: (\Dl,LI I\ e,m·J-ta-M.; /\_,teT\Wc --
_ Other (4) _ Other (8) --
R --
--
Organic Chemistry Inorganic Chemistry --
E Parameter Results(mg/1) Parameter Results(mg/') Ii,: gjlt~ Organic Compounds Results(mg/1)
· P&T:GC/MS . v Arsenic <o,ol benzene --
Acid:B/N Ext. V Barium <' 0, i carbon tetrachloride --
MTBE V Cadmium co.ooc chlordane
------
Chloride chlorobenzene ----
--. V Chromium (o. o l chloroform· --
I Copper .. o-cresol ------
. Fluoride ·-·· m-cresol ------
--Iron p-cresol ----
I --....iL Lead <aoo<:::: cresol --
--V Manganese tJ.. Q,\ --1,4-dichlorobenzene
~
--V Mercury o.oc.:-~:'l 1,2-dich loroethane --
I --(./ Nitrate 1, 1-dichloroethylene --Selenium
--
V L.o.cl 2, 4-dini trotoluene --
[/ Silver (.o.a.s:-heptachlor --
I Radiochemistry. Sulfates· hexachlorobenzcne ----
······-··-Zinc hexach lorobutadiene
Parumetcr
--
Results (PCi/1) "w< pH, hexachloroethane --
I
__ Gross Alpha --Conductivity __ methyl ethyl ketone
Gross Beta TDS nilrobcnzene ------
TOC pentachlorophenol ----
----pyridine
I Microbiology ----tetrachloroethylene
----trichloroelhylene
Parameter Results (Col/lOOml) __ 2,4,5-lriehlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --
I lindane
Date Received Reported by --mcthoxychlor --
--toxaphene
I 0~1lc ExtraclL:d 06i~forted 2,4-0
~ 20 AUG 2897 --_ 2,4,5-TP (Silvcx)
Dale Analyccd Lab Number --
I
I N.C. Ocpar1mcnt o( Environment,
I lea Ith, & Nalural Resources
Solid_ Waste Management-Division
SAMPLE ANALYSIS REQUEST State Ulboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Rakig.h, North Carolina 2761 l
~c Number Alco et;;; z__ ss.s 71 z.. Field Sample Number IQ( 7 L({) L
Name of Site S,@no/1.5 Sy?kc..-?4;1/c. Site Location SfdeJ Vi '( /e_
I Collected By J .j '::, ID# ___ Date Collected G/,__r., ( 17 Time / 0 3'S
I Agency: Hazardous Waste Solid Waste Vsuperfund
Sample Type
I Environmental Concentrate Comments
V Ground water (1) Solid (5) ?of{S t,U l( ( = Liquid (6fcJ/Z../ /ij /:-,{ /J(r-WA:ftfL I __ Surface water (2)
m
_ Soil (3) _ Sludge (7) _lt,--=---=!&LJ_;,:c___-f= _____ _
_ Other (4) _ Other (8) __ S._S.--__ 0_4'----'--P_L_c_J __ _
Organic Chemistry Inorganic Chemistry
D Pnrnmeter
P&T:GC/MS
.Acid:B/N Ext.
MTBE
Results(mg/1) Parameter
V Arsenic
V Barium
l/ Cadmium
Results(mg/'H a10 ill
<o,o r
I
Chloride
V Chromium
Copper
Fluoride
Iron
_k::.Lead
V Manganese
V Mercury
i/ Nitrate I V Selenium
r-----------------i V Silver
I Radiochemistry Sulfates
Zinc
Parameter Results (PCi/1) ~
__ Gross Alpha I Gross Beta
I Microbiology
1--------l
Para·rncter Results (Col/lOOml)
__ Conductivity
TDS
TOC
<0,1
(o. oo C
tJ, 0 ;J &
L. .Q,i:i._!;;_0..5
L.o • .c, I
I
I
Dale Received Reported by ------------------
1):, [ c Extraclcu Date Rcporled -----012121 ~u=·c~2=a '1~·7---
Dalc An»lyzcd Lab Number ----------~
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium,
Chromium
Lead
Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
p-cresol
crcsol
Results(mg/1)
Results(mg/1)
------
1,4-dichlorobenzenc __ .:..__ __ _
1,2-dichlorocthane
1,1-dichloroethylene _____ _
2, 4-dinitroto lucne
hcptachlor
hexachlorobenzcne
hexachl0robutadienc
hexachloroethan,e
methyl ethyl ketone
nilrobenzenc
pcntachlorophenol
pyridine
t e t.r acid oroet h ylene
__ trichloroethylene
__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol
vinyl chloride
endrin
lindane
melhoxychlor
loxaphcne.
2,4-0
2,4,5-TP (Silvcx)
------
I N.C. Department of Environment,
! !callh, l,t. Nalura\ Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 3()6 N. Wilmington Street
Raleigh, NOrth Carolina 27611
.. e Number ;VC.,L) ~ Z... SS5 7C/ Z... Field Sample Number (0 ( 7 ZG 3
Name of Site S,@?:]o/1..5 Scj:,·kc 72?,.;1/c. Site Location Sfq/e.s Vi //e....
I Collected By J fi ,z... ID# ___ Date Collected 0/zwMl Time (7Z..C3
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds
----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --Barium
V Ground water (1) /hCr1rf-i>r (j/d L u\1 .<; I k --Cadmium, Solid (5) --
D __ Surface water (2)
Chromium ss-os-c,w --
Liquid (6) Lead --Mercury --
I _ Soil (3) _ Sludge (7) Selenium --Silver
-... Other (4)
--
_ Other (8) --
I . --
--
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/') w o,118i Organic Compounds Results(mg/1)
_P&T:GC/MS v Arsenic <o, of benzene --
Acid:B/N Ext. V Barium 6, 8 car!Jon tetrachloride --
.V Cadmium MTBE (o, ooC chlordane ------
Chloride chlorobenzene
----
--V Chromium 0, o ·J.. chloroform --
I --Copper o-cresol --
'" -. .-. ·---·-. Fluoride m-cresol ------
--Iron p-cresol --
I --_1L::.Lead t?, 0 i-;J crcsol --
--V Manganese It,' fl_ t3. --1, 4-dichlorobcnzene
--V Mercury 0-<c>:J --1,2-dichlorocthane
I --V Nitrate 1, 1-dichloroethylene ----
V Selenium <-o, al 2, 4-d;ni trotoluene --V Silver < /)_, 0~ --heptachlor
I Radiochemistry Sulfates hexachlorobenzene ----
······-·· Zinc hexachlorobutadienc
Parameter ----
Results (PCi/1) ~ pH ~ hcxachloroethane --
ii __ Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC pent_achlorophenol ----
----pyridine
I Microbiology ----tctrachloroethylene
__ trichloroetloylene --
Panunctcr Results (Col/lOOml) __ 2,4,5-triehlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --
I lindane
Date Received Reported by
--mctr.oxychlor --__ toxaphcne
I D:itc ExtractcJ Dae Rcf\J!ited 2,4-0
1.2 ~2 AUG2597 --
I
2,4,5-TP (Silvcx)
D:itc Analpcd Lah Number
... -. .. ,. ' . ~ '".' --
I, N.C. Ocp<H1mcnt o{ Environment,
1 lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 t-.'. Wilmington Street
Raleigh, North Carolina 27611
.. e Number NC)) C0 Z-SS5 7C/Z-Field Sample Number 0(7 ·z<of
Sfx!esVI l/e... Name of Site ~r r St:fkc_ 7411/c. Site Location _ @no/IS
I J ef__--z.(p L1 J Collected By jS ID# Date Collected Time /3/o
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds
----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --Barium
V Ground water (1) (/,1<:Yt 1:+or we(/ --
_ Solid (5) Cadmium --
~ om , · 1:e--[J tw ( 1 s if\
Chromium
__ Surface water (2)
--
_ Liquid (6) Lead --
SS -00 ~ 6UJ --Mercury
D _ Soil (3) _ Sludge (7) Selenium --Silver
_ Other (4)
--
_ Other (8) --
I --
--
0 rga n ic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/') ( g;'lt, Organic Compounds Results(mg/1)
_ P&T:GC/MS v Arsenic ?b.1 1 benzene --
I
t= Acid:B/N Ext. V Barium carbon tetrachloride
V Cadmium
--
MTBE < l>,oor chlordane ----
Chloride chlorobenzene
----
V Chromium --( c::?. o I chloroform --
I --_·_Copper o-cresoi --
Fluoride m-crcsol ------
Iron --
p-cresol
I --....k::. Lead <tJ. ()0£ crcsol --
--V Manganese (I!, D3 1,4-dichlorobenzene --
--v Mercury L... 0 -CC;, ,-:J .5 1,2-dichloroethane
I --v Nitrate __ 1,1-dichloroethylcne --V Selenium "'-.Q.Oj 2, 4-dinitrotoluene --V Silver <1J, oS-heptachlor --
I Radiochemistry Sulfates hexachlorobenzene ----
······-·· Zinc hcxachlorobutadiene
l)arametu Results (PCi/1) ----
--0 pl! hexachloroethane
I
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
--Gross Beta TDS nitrobenz.ene --TOC __ pentaehlorophenol --
--__ pyridine
I Microbiology --__ tetrachloroethylene
__ trichloroethylene --Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----_. _2,4,6,trichlorophenol
------vinyl chloride
endrin --
I lindane
Date Received Reported by
--methoxychlor --
--toxaphene :
I D:1tc Extracicd D l} f:?o fJ,<;d, 0 2,4-D --~:ti,.;..:: AUG 2u 97 _ 2,4,5-TP (Silvcx)
Detlc Analy,cd Lah Number --
I i'-!.C. Department of Environmcnl,
I lcahh, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
s-55 7qz._ Field Sample Number
State Labora1ory of Public Health
P.O. Box 28047, 3()6 N. Wilmington Street
Raleigh, North Carolina 27611
0177-bS ~le Number Alco ~ z....
Name of Site c._,r I ljrno/lS Scf-kc.. ?a/lie.. Site Location Sf qj-es VI //e_
I Collected By JS ID# Date Collected <aLzs(ql Time (SI S
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds
----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
Be{otAJ
Barium
p?6 ·--
__ Ground water (1) _ Solid (5) Cadmium --
I · V Surface water (2) ss-07 -s.w Chromium --
_ Liquid (6) Lead --__ Mercury
I _Soil (3) _ Sludge (7) Selenium --Silver --
_ Other (4) _ Other (8) --
--g --
Organic Chemistry Inorganic Chemistry --
n Parameter Results(mg/1) Parameter Res~lts(mg/1)(~ Organic Compounds Results(mg/1)
P&T:GC/MS V Arsenic < (l, QI benzene ----<o,/ --_ Acid:B/N Ext. I_,, Barium carbon tetrachloride --
MTBE ~ Cadmium < o. oo< chlordane ----Chloride chlorobenzene ----?o, or --
--_LL:. Chromium chloroform --
D --__ Copper o-cresol --
--Fluoride m-cresol ----
--Iron __ p-cresol --?o, oo,C
D --;__,.-Lead cresol ----
--l./Manganese ()_, 'J.I. --1,4-dichlorobenzene
v Mercury L....0-bc.""--.c.:.-,,;5 1,2-dichloroethane ----
--v· Nitrate __ 1,1-dichloroethylene
E --v ·Selenium L_CJ_ cl 2,4-dinitrotoluene --v Silver <o, o < heptachlor ----
Radiochemistry Sulfates hexachlorobenzene ----i ...... _ .. _ Zinc hexachlorobutadiene
Parameter ----Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Bela TDS nitrobenzene ----TOC __ pentachlorophenol --
--__ pyridine
I Microbiology --__ letrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --G= --__ 2,4,6-trichlorophenol
--vinyl chloride --endrin --lindanc
I Date Received --Reported by __ methoxychlor
__ toxaphene
Date ExlracteJ Dale Reported 2,4-D --I ~t::;f.2,,: AUC 2897 __ 2,4,5-TP (Silvex)
Date Analy,cd ,ab um5cr --
DllS J!1Jl (!lcviscd 2/91)
" .~-C. Dcp::1r1mcn1 of Environment,
D I lcahh, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
D .le Number IVCO a(; z._ sss 7C/ 2... Field Sample Number of 72GG
Name of Site y@no/7..S Sy?·kc.... 7a,/t/c.. Site Location Sfd-e,s//i //e_
g Collected By J ---J S, ID# Date Collected '2J/-z.-S/ 01 Time /4'[)0 ll ----I
Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
m
Environmental Concentrate Comments Arsenic --
&c.):;~J n2 u -rl Barium --
__ Ground water (1) _Solid (5) Cadmium --Chromium
I Vsurface water (2) Pot1,d --
_ Liquid (6) Lead --I __ Mercury
_ Soil (3) Sludge (7) S~~ Cf() -f?tl, S,L.u Selenium --I Silver
_._ Other ( 4) --_ Other (8) --
--
I --Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/1; _,w,ftill! Organic Compounds Results(mg/1)
_ P&T:GC/MS (....--Arsenic <o, 0 I benzene ----Acid:B/N Ext. v Barium fg:&;,c carbon tetrachloride
MTBE v-Cadmium
--chlordane ------
Chloride chlorobenzene ----<o,or --
--...i..e:_ Chromium chloroform --
--__ Copper o-crcsol
I --
--Fluoride. m-cresol ----Iron __ p-cresol ----<o, OQJ~ --L--Lead cresol ----I --. ___5::::_ Manganese D, of. 1,4-dichlorobenzene --
--_!::::._ Mercury .L...C> ,_ c:::. c-.,c-.5 1,2-dichlorocthane
L-Nitrate __ 1,1-dichloroethylene --c:::--I Selenium ..t:...O-Ci 2,4-dinitrotoluene
~Silver <&,DC --heptachlor ----
Radiochemistry Sulfates hexachlorobenzene ----
I n••••-•• Zinc hexachlorobutadiene
Parameter ----Results (PCi/1) pH · hexachloroethane ----__ Gross Alpha Conductivity __ methyl ethyl ketone --
I Gross Beta TDS nitrobenzcnc ------
--TOC __ pentachlorophenol
pyridine ----
I
Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Paramfter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
--.. vinyl chloride -----endrin --lindane --Date Received Reported by I __ mcthoxychlor
__ toxaphene
D:ilc Extracted Dale Rc~rtcd 2,4-D --
I 01;~1 .. ::: AOG2u·1/ 2,4,5-TP (Silvcx)
Dale Analy,cd Lab Number
DI IS 3!1Jl (IZcviscd 2/91) --
' N.C. Department of Environment, I I lcalth, & Natufal Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
sS5 717... Fie.Id Sample Number
State Laboratory of Public Health
P.O. Oox 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
(.)( 7 z_.(;, 7 •• le Number-'-M-'-'c.=o<--=-X=-=Z---==---==---:__,__-
c .r I Name of Site Yjrl'l0/1 S S<f-li'c 7a,Alc. Site Location Sides Vi '//e_
I .Collected By __ ~_j=-..cS,~----ID# Date Collected ~?-S[,r/ Time !?,to
I Agency: Hazardous Waste Solid Waste Vs uperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
i?PckJro~
Barium --
__ Groundwater (1) Solid (5) Cadmium --Chromium g V Surface water (2) pere,c/l.itJ '\1o i.'vll\. --_ Liquid (6) Lead
__ Mercury
_Soil (3) _ Sludge (7) SS.-Ot)-SVJ Selenium
0 --Silver
_ Other (4) --_ Other (8) --
--
D --Organic Chemistry Inorganic Chemistry --
.
E Parameter Results(mg/1) Parameter Results(mg/1) ( g;flR) Organic Compounds Results(mg/1)
_P&T:GC/MS L.---' Arsenic <o,o I benzene --Acid:B/N Ext. --1L Barium <o,t carbon tetrachloride --MTBE V Cadmium (0,60 J chlordane ------Chloride chlorobenzene ----
--G Chromium <o,o £ chloroform --• --__ Copper o-cresol --.. Fluoride m-cresol .. ------Iron p-cresol ------
--v Lead <0.00,1----cresol --I --V Manganese <o,o:r 1,4-dichlorobenzene --
--V,.. Mercury .£-.Q-~c:..o-5 1,2-dichloroethane
L-Nitrate __ 1,1-dichloroethylene --
I i,-· Selenium <.Ci -C ) 2,4-dinitrotoluene
l-/ Silver --<c2,o.C heptachlor ----.. Radiochemistry Sulfates hexachlorobenzene ----
I ······-··-Zinc hexachlorobutadiene
Pararnt:ter ----Results (PCi/1) pH hexachloroethane ----__ · Gross Alpha __ Conductivity methyl ethyl ·ketone --
I --Gross Bela TDS nitrobenzene ----
--TOC __ pentachlorophenol
--__ pyridine
I Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichJorophenol
------vinyl chloride
endrin --lindane --
I Dale Received Reported by __ methoxychlor
--toxaphene
D:ilc ExtracteJ Dale Reported 7 2,4-D --
I 01':12:S ~UC 2o9 2,4,5-TP (Silvex)
Dale Analyzed Lab Number
1)1 IS )l1JI (l~cviscd 2/91) --
I N.C. Department of Environment,
1 lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Dax: 28047, 306 N. Wilmington Street
Ralcig.h, North Carolina 27611
•• le Number Alco Ct;; 2.-sss 7'1 Z...
N.ame of Site S,3mo// .5 $:'f-h 'c ]'a;t /c.
Field Sample Number O (7-Z.. (,, 'f3
Site Location SftJJ-es //1 //e__
. I Collected By b fl_;\ ID# Date Collected 9(21,o(o/l Time O'i3 4)
I Agency: Hazardous Waste Solid Waste Vs uperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
[}J,v i 4Sb(I ?00<£ Barium --
__ Ground water (1) _ Solid (5) Cadmium --Chromium
I V Surface water (2) ':::, -::,~ ( 0 -SW --
_ Liquid (6) Lead --__ Mercury
_ Soil (3) _ Sludge (7) Selenium
I --Silver
_ Other (4)
--
Other (8) --
--n --
Organic Chemistry Inorganic Chemistry --
n Parameter Results(mg/1) Parameter Results(mg/I)t,. g;'IIII) Organic Compounds Results(mg/1)
_ P&T:GC/MS V Arsenic <o,o 1 benzene --
Acid:B/N Ext. L, Barium o,t carbon tetrachloride --
--MTBE <--Cadmium <o, ooS:::: chlordane ----Chloride chlorobenzene ------
--(._,, Chromium (,2, o I chloroform --
n --_·_ Copper o-cresol --
--Fluoride m-cresol ----Iron __ p-cresol --
--V L<:ad < 0, !Jo,C cresol u --
--V Manganese Ci-J?: 1,4-dichlorobenzcne --
--V Mercury -c:...o .. c::=::.c:.o ;5 1,2-dichlorocthane --
--v Nitrate __ 1,1-dichloroethylene
n v Selenium ~a. Cl .. ·· 2,4-dinitrotoluene
V Silver <a,o.r --__ heptachlor
Radiochemistry Sulfates hexachlorobenzene ----
0 •n•••-••--• Zinc hexachlorobutadiene
Parameter ----Results (PCi/1) _pH hexachloroethane --__ Gross Alpha _·_· _ Conductivity __ ·· methyl ethyl ketone ..
n --Gross Beta TDS nitrobenzene ----TOC __ pcntachlorophenol --
--__ pyridine
0 Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --lindanc --D Dote Received Reported by . __ methoxychlor
__ loxaphene
Date Extracted Dale R~orted 2,4-D 0121 ~, A' ?'197 --
0 I.. I , •. _Q __ 2,4,5-TP (Silvex)
Dale Analy1.ed Lah Number
l)l!S J[<JJ (llcviscd 2/91) --
I N.C. Department of Environment,
I lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboralory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
•• le Number_.:_M...:...:::c:...b'-=-G0~Z....=------=s:..._S--=5-7-'----'-C/_Z... ___ Field Sample Number ____ 0.=....,(_7J..c2-,c_r;,,_cz,__ ____ _
Name of Site Si3mo/1S Stp-kc.. 7?<.;1/c.. Site Location _ ___,Ss..,_:_i=.¼2.o"'---'Vc.cl~/'---'~c.,:L=----------
1 Collected By i)/1;/ ID# ___ Date Collected_0_/_2-_G---'(.~q-'--'7 ____ Time Cfo'Zo
I Agency: Hazardous Waste Solid Waste Vs u pe rfun d TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --·o 0-, <J I , C( '.y_5Y\ f)J'h._~
Barium --
__ Ground water (1) Solid (5) Cadmium --I Chromium I V Surface water (2) "(). c) f) I I Cfo~ . --
_ Liquid (6) Lead --I __ Mercury
_ Soil (3) _ Sludge (7) SS-//o -s1,-0 Selenium
I --Silver --_ Other(4) _ Other (8) --
--g --
Organic Chemistry Inorganic Chemistry --
g Parameter Results(mg/1) Parameter Results(mg/1\ Iii si'..i Organic Compounds Results(mg/1)
_P&T:GC/MS L-,--Arsenic <o,O/ benzene --Acid:B/N Ext. _L::,_ Barium 0, '.) carbon tetrachloride --
MTBE v Cadmium ( ,1 ,QOJ_.--chlordane ------Chloride chlorobenzene ------
--L.--Chromium IJ, D I -chloroform ----
n --Copper o-cresol ----
--Fluoride m-cresol ----Iron __ p-cresol ----
--..J..c:.... Lead ~.01, cresol
0 --
--\.,.,"'"" Manganese L, 'J~ --1,4-dichlorobenzene
v Mercury .e...._q_ot:>b5 1,2-dichloroethane --
--L,,' Nitrate __ 1,1-dichloroethylene
D 1../ Selenium L..Q-01 2,4-dinitrotoluene
V Silver --(o.o C heptachlor ----
Radiochemistry Sulfates hexachlorobenzene ----
0 ······-··-Zinc hexachlorobutadiene
Parameter ----Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity methyl ethyl ketone --
D Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol --
--__ pyridine
0 Microbiology --__ tetrachloroethylene
---__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl.chloride
endrin --lindane --D Dale Received Reported by __ meihoxychlor
toxaphene
D:.il~ Ext raclcd --0 't'J°1~~o~~ AUG 2597 2,4-D --
E 2,4,5-TP (Silvcx)
Date Analyzed Lab Number
l)J!S 1JIJ1 (llrvi,;,'.d 7/1/1' --
' .
fl' N.C. Department of Environment, II I lcalth, & Natura! Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
sS5 717-Field Sample Number
State Laboratory of Public Health
P.O. Box; 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
0(7Z.70 llete Number /VC:,Q C0 2-.
Std-es //1 l /e__ Name of Site <:__;' ( sqzn·c.-74/1./c_ Site Location ljrno11s
I Collected By 0/41 ID# Date Collected 'Bl zs! c:;1 Time ("SIS
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
I · Environmental Concentrate · Comments Arsenic --
<;. --fr e_,:;fvl
Barium
T;,-rf --
__ Ground water (1) _ Solid (5) Cadmium --
I l.,u psf-cP ~;.i-fz.. Chromium
V Surface water (2)
--
_ Liquid (6) Lead --
ss~ 1 b ~ s1.,,u __ Mercury
I _ Soil (3) _ Sludge (7) Selenium --Silver
_ Other (4)
--
_ Other (8) --
I --
--Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/l)f m'!ltl Organic Compounds Results(mg/1)
_ P&T:GC/MS V Arsenic <o.o( benzene
Acid:B/N Ext. V Barium
--<o, t carbon tetrachloride --v Cadmium MTBE < 0, 00-,) chlordane ------
Chloride chlorobenzene ----< o, 0 i --
--v Chromium chloroform --
I ----Copper --o-cresol
--Fluoride m-cresol ----
--Iron __ p-cresol --< o. I --V Lead DD-L cresol --
--v Manganese 0., t2. ' --1,4-dichlorobenzene
v Mercury L...c, _~,":>C>S 1,2-dichloroethane ----
--/../ Nitrate __ 1, 1-dichloroethylene
I lL.__ Selenium ""'-c., • Q l --2,4-dinitrotolucne
l/ Silver (o,os: heptachlor ----Radiochemistry Sulfates hexachlorobenzene
I ----
··"··-·· Zinc hexachlorobutadiene
Paramekr ----Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone
I --Gross Beta TDS nitrobcnzenc ----TOC __ pentachlorophenol --
--__ pyridine
I Microbiology --__ tetrachloroethylene
--__ trichloroethylene ·
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --lindane
I Date Received Reported by --__ methoxychlor ·
-__ toxaphenc
D:.ilc. ExlractcJ Dlltc Re1orted () 97 2,4-0
I --01c:: '19 .a:uc 2 _ 2,4,5-TP (Silvcx) A.. .L.
Dale Analyzed Lab Number --I) I p.,: 1. !l!I / 11 ,..,;,.,.,I ? /LI I)
·' . ' :--.:.c. Dcp;inment of Environment,
1 !c;illh, & Natural Resources
Sulid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Strect
Raleigh, North Carolina 27611
.. ilc Num ber_;_IVi.:..,L-cc:;0,L. -=(X;-=-=Z..=----s=---S-=5___:7~1,_2... __ _
Name of Site S(3rno/l ..S sqzn 'c... ffi/l /c..
Field Sample Number 6(7 -Z.. ·7 (
Site Location Sfci.Jes VI //e.....
I Collected By JS, ID# Date Collected <o/z.s / "I 1 Time [7 2,S
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
(JJ 1 {( ltl./V\5 JYY\c(
Barium --
Ground water (1) _ Solid (5) --Cadrniu'!'
I Chromium
I V Surface water (2) Ss-,-11~sw --
Liquid (6) Lead ----Mercury --
Soil (3) _·_ Sludge (7) Selenium ----
I Silver --
_ Other (4) --Other (8) --
--
I --
Organic Chemistry Inorganic Chemistry --
I Parumeter Results(mg/1) Parameter Results (mg/I) V§)"-it\ Organic Compounds Results(mg/1)
_ P&T:GC/MS V Arsenic <o, ,2 I benzene
v Barium --
_ Acid:B/N Ext. < o, / carbon tetrachloride ----
MTBE v Cadmium <o. oo C chlordane ------
Chloride ·--·-.. . •"· --chlorobenzene ------( V Chromium {), () ( chloroform ----
--__ Copper o-cresol
I --
--Fluoride m-cresol ----
Iron __ p-cresol ----i./ Lead (11, 40 C cresol ----
I --!.-'"""" Manganese (), tJ':f. --1,4-dichlorobenzcnc
--C/ Mercury < ()_, 12.o.c::i r --1,2-dichloroethane
v Nitrate __ 1,1-dichloroethylenc ------
I V Selenium L..c, -ci;;,... 2,4-dinitrotol ucne --J...L Silver < ,:2., l2, (---heptachlor
Radiochemistry Sulfates hexachlorobenzene ----
I ..... -, .... Zinc hexach lorobut adiene
Parameter --pH . --
Results (PCi/1) hexachloroethanc ----
__ C:Jrnss Alpha __ Conductivity __ methyl ethyl ketone
I Gross Beta TDS nitrobenzcnc ------
TOC __ pentachlorophenol --
--__ pyridine
I
Microbiology --__ tetrachloroethylene
--__ trichloroethylenc
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophcnol
----vinyl chlorid~ --
endrin --lindanc --
Date Received I Reported by --methoxychlor
--toxaphcne
D:itc Extr:ictcJ Dale Revorted . 2,4-D
012130 AUG 2f>; 7 --
I __ 2,4,.\-TP (Silvcx)
Ddlc /\n;ily1.cJ Lab Number
l>I IS .'l'JI (llcvi~cd 2l1\)
--
. '
I N.C. Dcpa11mcnt of Environment,
I lea Ith, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
s-S5 7C/Z.... Field Sample Number
State Laboratory of Public Health
P.O. 13ox 28047, 306 N. Wilmington Street
Raleigh, North Carolina 2761 l
0(777?..
.. e Number NC,Q C10 Z-
Sfds;.s Vil /e.-Name of Site ~r I Syz·kc 7?{..;1/c.. Site Location _ 6ftlo/1S
I Collected By
J
/. z__ ID# Date Collected Y._ 2.-s[ ci'l Time /&,/ 8
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds
----
Sample Type Inorganic Compound., Results(mg/1)
I Environmental Concentrate Comments Arsenic --Barium
V Ground water (1) Si5/Y\(>!\ we l/ --Cadmium. Solid (5)
I
--Chromium
"E-brz.-1µ1c..-1 Al c, --
__ Surface water (2) _ Liquid (6) Lead --
WA-1e:ri w8.J..,'f----Mercury
I _ Soil (3) _ Sludge (1) Selenium --Silver
S,'3,-·?:,--z_. -!:::,W --
_ Other (4) _ Other (8) --
I --
--
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/1)~ Organic Compounds Results(mg/1)
_ P&T:GC/MS v Arsenic :?~:? t
benzene --
Acid:B/N Ext. V Barium carbon tetrachloride --
V Cadmium ~-MTBE <o. oo,s= chlordane ----
Chloride chlorobenzene
--<'.o, o I --
--V Chromium chloroform
0
--
--_·_Copper o-cresol --
Fluoride m-cresol ------
--Iron p-cresol --
D --....k:::. Lead < o, oo,C cresol --
--V Manganese <o, D°1' 1,4-dichlorobenzene --
--V Mercury ZQ.()l'.QQ 1,2-dichloroethane --
0 --V Nitrate 1, 1-dichloroethylene ----
V Selenium ~c:>-c3, · 2,4-dinitrotoluene --V Silver s:: f2., Q s---heptachlor
D Radiochemistry Sulfates hexachlorobenzene ----
""··-··-Zinc hexachlorobutadiene
Paramder
----
Results (PCi/1) ~ hexachloroethane --
D __ Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene
------
TOC pcntachlorophenol ----
E ----pyridine
Microbiology ----tetrachloroethylene
..
--__ trichloroethylene
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-tricWorophenol
----vinyl chloride --endrin --
I .. lindane
Date Received Reported by
--methoxychlor --
--toxaphenc
I D:itc Extracted 61°:ftP.''f ct . -2,4-D
"· _; UC 28 9 7 --_ 2,4,5-TP (Silvcx)
Date An;,l)nd Lab Number --
:-.:.C. Dcp::irtmenl of Environment,
! k::ilth, & Natural Resources
Sulid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
D
0
u
.itc Number NC,L) {)(; 2...-
<::_:;' r
ss.s 717-Field Sample Number 0(72-73
74;1/c.. s1c)__&:.s vr l /e__
I
I
I
I
I
I
I
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I
It
I
I
Name of Site St'fz-·ke-Site Location ~rno/1 s
Collected By bw ID# Date Collected <o(¼(Cfl Time (]2..-S
Agency: Ha,.ardous Waste Solid Waste Vsuperfund TCLP Compounds
----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --. Barium
Posf--Presenf=<-1'i'ue.. --Cadmium
__ Ground water.(l) . Solid (5) --
BIA(\,t
Chromillm
_ Liqu~d (6)
--
__ Surface ·water (2) Lead --
ss-/oo -PB
__ Mercury
_ Soil (3). _ Sludge (7) Selenium --. Silver --
.Ji Other ( 4) _ Other (8) --
--
--
Organic Chem~stl)'. .. Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/11 .. s:fl a) Organic Compounds Results(mg/1)
_ P&T:GC/MS V Arsenic <o,D L benzene --
..iL. Barium Acid:B/N Ext. (:.o., i --carbon tetrachloride
--MTBE V Cadmium < 0,00,.l chlordane --
Chloride chlorobenzene
------
--V Chromium <o. QI chloroform --
--Copper o-cresol ----
Fluoride m-crcsol
------
--Iron __ p-cresol
--v Lead <cJ, ~if cresol
-C:, Manganese
--
--< D., --1,4-dichlorobenzcne
--er-Mercury L_Q.,: ,'"::.>.c.-..,--5 --I, 2-dichloroethane
--Nitrate __ 1,1-dichloroethylene
.:;;,-Selenium ..C:.o.c\-2,4-dinitrotoluene --
l/ .. Silver < ll, oS: __ heptachlor --
Radiochemistry Sulfates hcxachlorobenzene
----
······-····--· Zinc hexachlorobuladiene ----
Parameter Results (PCi/1) _pH hexachloroethane
__ Gross Alpha __ Conductivity = methyl ethyl ketone
Ciross Beta TDS nitrobenzene
------
TOC __ pcntachlorophenol --..
--· __ p)'Tidine
Microbiolo.gy --__ tetrachloroethylene
__ trichloroethylene
.
--
p_aramL·lt'.r Results (Col/!00ml) __ 2,4,5-trichlorophenol --
----2,4,6-t richlorophenol
, = ,inyl chloride
----' ; endrin --
J lindanc
Date Received Reported by __ methoxychlor
... __ toxaphcne
l);itt: Exlractt.:d D 'ij l'.l'i._' rt c·d 2,4-D
L J2-AOG 2597 --__ 2,4,5-TP (Silvex) i
Dale Analy1ed Lab Number I
llllSJl'JI (llc\·i~cd ~/WI)
--. I
' .
I N.C. Depanmcnt of Environment,
! !calth, & Natural Rcs.ourccs
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST Stale Labof'll.tory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
.. e Number ;VC,Q Ct;:; Z... SS5 712... Field Sample Numbcr ____ 0_/_:7_z._-_7_,i-____ _
Name of Siie_Si"'-IJ"I-' _m.c.co~/1--'S"--
1 ~Yf==i,::._f,__c•c...c..-~P~~/1~f_c.._ Site Location_...,'--Sc...f d-e.r-'-=--'-1/'.-'-/ -'-'(.,_/e_=----------
1 Collected By ____ ~~s;, ____ ID# ____ Date Collected. __ 0_,_/_?.._w_· -"-{u....:(_I ____ Time __ /_s_· l_o _ _;__
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds
----
Sample Type Inorganic Compound., Results(mg/1)
I Environmental Concentrate .. Comments Arsenic --
la._ «Jx' 1-h
Barium
V Ground water (1) u·c I/ --Cadmium. Solid (5) --
I __ . Surface water (2) thiU /J ~( N Lt
Chromium --
Liquid (6) Lead --
()J ft-7 [:fl {_y{_-{l,:'f --Mercury 1-· Soil (3) _ Sludge (1) Selenium --Silver
S S -""., 3 -PL,u --
_ Other (4) _ Other (8) --
I --
--
Organic Chemistry Inorganic Chemistry --
I Pam meter Results(mg/1) Parameter Results(mg/') (: g;'PI, Organic Compounds Results (mg/I)
_ P&T:GC/MS v Arsenic < D, O i benzene --
Acid:B/N Ext. V Barium <o, I carbon tetrachloride --
MTBE V Cadmium ( t?, Do,£ chlordane
------
Chloride chlorobenzene
------
--V Chromium ( o. o / chloroform --
I --_·_ Copper o-creso! --
Fluoride m-cresol ...
------
--Iron p-cresol ----
I --_[LLcad (), a I?-: cresol --
--V Manganese < Q, o:1 1,4-dichlorobenzene --
--V Mercury .L..o .. Dor.~~ 1,2-dichloroethane --
I --v Nitrate 1,1-dichloroethylene ----
V Selenium <..,Q -Q\ 2,4-dinitrotoluene
·v Silver <o.o,r --
--heptachlor
I Radiochemistry Sulfates . .. ·' hexachlorobenzene ----
······-·· Zinc hexachlorobutadiene
Parameter Results (PCi/1) ----
,.-" pll hexachlorocthane --
I
__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS hitrobcnz.ene ------
TOC pentachlorophenol ----
----pyridine
I Microbiology ----tetrachloroethylene
--__ trichloroethylenc
Parameter Results (Col/lO-Oml) __ 2,4,5-trichlorophenol
-~
--__ 2,4,6-trichlorophenol --
----vinyl chloride
endrin --
I lindane
Date Received Reported by
--methoxychlor --__ toxaphene
I D:itc ExtractcJ D a IITTJ'Wti:dc;· 2,4-D
AUG za9; --_..._lJ~ 2,4,5-TP (Silvcx)
D,1tc Analyzed Lah Number --
I
• • N.C. Department of Environment,
1 kalth, & Natura! Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State l.abora1ory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
•• e Number_..:M~c""o~~-=-:z_=-----=s:...;S:..:5=-------'-7_1c_c..2-___ Field Sample Number o/7 2-75
Name of Site ':J6;'rn0/1.5 Vn7l'C-76;1/c... Site Location Sfd-ey //i / /e_
I J =,:--/,
Collected By ____ ~=.S~---ID# ___ Date Collected 0(',zc,,~q 1 Time / S1:o
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds
--
Sample Type Inorganic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
Ie,1fle.1 lue((
Barium
V Ground waler (1)
--
Solid (5) Cadmium --
I .(;._ T)/?..l ltJ Kl Iv lr
Chromium
__ Surface water (2) Wft{eK---
_ Liquid (6) Lead --
UJ Eu.., t---Mercury
I _ Soil (3) _ Sludge (1) Selenium --Silver
_ Other (4) ss -?:.>4--?vJ --
_ Other (8) --
I --
--
Organic Chemistry Inorganic Chemistry --
I Pura meter Results(mg/1) Parameter Results (mg/I)~ Rl'I~ Organic Compounds Results(mg/1).
_ P&T:GC/MS v Arsenic <o,o I benzene --
_ Acid:B/N Ext. V Barium (o, i carbon tetrachloride
I
--
MTBE V Cadmium :< o, oo,C chlordane ------
Chloride chlorobenzenc
--< Q, i) /
--
--V Chromium. chloroform --
I _·_Copper .. o-cresol
----
--Fluoride m-cresol. ----
--Iron p-cresol --
I --__k::. Lead < tJ, Oo.C cresol --
--V Manganese D,O;, 1,4-dichlorobenzene --
--V Mercury L...c, _ .. :::.<::><'-=>;$ 1,2-dichloroethane --
I --V Nitrate 1, 1-dichloroethylene ----
V Selenium <.0-~i 2,4-dinitroto luene --
[./ Silver <o, DC --heptachlor
I Radiochemistry Sulfates hexachlorobenzene
----
······-··-Zinc hexachlorobutad iene
Pi.Jrameta ----
Results (PCi/1) ...,-rll hexachloroethane
I
__ Gross Alpha __ Conducti;,,;ty __ methyl ethyl ketone ·
--Gross Beta TDS nitrobenzene --T0C __ pentachlorophenol --
----pyridine
I Microbiology --tetra chlo roe thylene --
--__ trichloroethylene
Paran1der Results (Col/lOOml) --__ 2,4,5-trichlorophenol . -'•
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --
I lindane
Date Received Reported by
--methoxychlor --
--toxaphcnc
I D:itc Extracted 0 fff .. Yfj;1 AUG 2597 2,4-D --_ 2,4,5-TP (Silvcx)
DJIC Analy1.cd Lah Number --
D
I } r I
;,,;::,!:_ Dcp:inmrnt of Environment,
llt.:allh, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
D .itc Number A/C,L) D{;; 2..-S"S5 71 Z...
Name of Site S-j:rno/1..5 St:f-h'c 72i.;1/c..
Field Sample Number O /7 -Z 70
Site Location Sf q../-es VI //e__
m Collected By S, ID# Date Collected '511...S( 11 Time ('rf2 0
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Agency: Hazardous Waste Solid Waste Vs u pe rfun d ------
Sample Type
Environmental Concentrate Comments
Ground water(!) _ Solid (5) &!_ow [cl(h be_,~
V Surface water (2) _ Liquid (6) p(JY\J
Ss-1/ro-Soil (3) Sludge (7) SVJ ----
Other (4) _ Other (8)
Organic Chemistry Inorganic Chemistry
Parameter Results(mg/1) Parameter Results(mg/l);jj-I (f,gt
--P&T:GC/MS V Arsenic (<2,0{ --
--Acid:B/N Ext. v-Barium ('o, i < 0, oo r::: MTBE V Cadmium --Chloride ----<o,D I --v Chromium
Copper ----Fluoride -----Iron ----(6.ou-C --V Lead
--_'::'._ Manganese i?,o·i-
v Mercury L.. o_"" ,-,, r:,..'.5 --L, Nitrate --v Scleniu.m ..L..n_cl
(/ Silver <o.QS-
Radiochemistry Sulfates --···········-·------Zinc --l'aramt'ler Results (PCi/1) _pH
__ (Jross Alpha __ Conductivity
Gro.ss Bela TDS ----TOC --
--Microbiology --
--Paraml0l1.:r Results (Col/lO0ml) --
----
----
Date Rcccivcd Reported by
D:lli.: Extr;1c1cJ 0 tft~Ij~ AUG 28 'ff
Dale An:tly-1.cd Lah Number
I JI l.'i .11 'JI ( l{(;\'i.\cd 2/') l J
TCLP Compounds
Inorganic Compounds Results(mg/1)
Arsenic --Barium --
--Cadmiur,i
Chromium --Lead --__ Mercury
Selenium --Silver --
--
--
--
--
Organic Compounds Results(mg/1)
benzene --carbon tetrachloride --chlordane --chlorobenzene --chloroform --o-cresol . --m-cresol --__ p-cresol
cresol --1,4-dichlorobenzene --1,2-dichloroethane --__ 1,1-dichlorocthylenc
2,4-dinitrotolucnc --__ heptachlor
hcxachlorobenzene --hexachlorobutadiene --hexachloroethane --__ methyl ethyl ketone
nitrobenzene --__ pentachlorophenol
__ . pyridine
__ tetrachloroethylene
. __ trichloroethylene
__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol
vinyl chloride --
' endrin --
lindanc --methoxychlor --toxaphenc --2,4_.D: --2,4,5-TP (Silvex)
--
--
I N.C. Department of Emironment,
l lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
s-S5 712... Field Sample Number
State Laboratory or Public Health
P.O. Box 28047, 306 N. Wilmington Street
RBleig.h, North Carolina 27611
0(7-Z-77 ... c Number NCQ Of;; Z...
Name of Site C/ I sqzn·c.-7"a.;1/c.. Site Location Sid-es(/( lie... _ tt?:30/IS I J e/zw {_47 Collected By J ID# Date Collected Time 134-D
I Agency: Hazardous Waste Solid Waste Vsuperfund
I Environmental
Sample Type
Concentrate
~Groundwater (1) _ Solid (5)
I __ Surface water (2) _ Liquid (6)
I Soil (3) _ Sludge (7)
j Other (4) _ Other (8)
Comments
E1v1//Yle;,,+ r/~/\~
bia"l-
1.-------.....--------1
Organic Chemistry Inorganic Chemistry
I Parameter Results(mg/1) Parameter Results(mg/1).
I
_ P&T:GC/MS
_ Acid:B/N Ext.
MTBE
v Arsenic
V Barium
V Cadmium
Chloride
V Chromium
Copper
Fluoride
Iron
I _L Lead
V Manganese
V Mercury
l/ Nitrate I V Selenium t----------------1 V Silver
I Radiochemistry
Parameter Results (PCi/1)
Sulfates
Zinc
_£pH
&.OJ
(O,ol
< D,o3
<o,oC
__ Gross Alpha ______ _ I Gross Beta
__ Conductivity ______ _
TDS
TOC
I Microbiology
1-------l
I
I
Parameter Results (Col/lOOml)
Date Reccivcd ___ _c ____ Reported by _________ _
Dcite Extracted Date R;jlorted -----u1.21r-T:1~0,~: A~u~c =2s~9=7~
D;ite Analyzed Lab Number
1)1 IS JJ!Jl (ltcviscd 2/9\) ----------
TCLP Compounds
Inorganic Com pounds
Arsenic
Barium
Cadmium.
Chromium
Lead
__ Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform·
o-cresol
m-cresol
__ p-cresol
cresol
1,4-dichlorobenzene
1,2-dichloroethane
Results(mg/1)
Results(mg/1)
------
------
__ 1,1-dichloroethylene _____ _
2,4-dinitrotoluene
__ heptachlor
hex.achlorobenzene
hexachlorobutadiene
hexachloroethane ------
__ methyl ethyl ketone _____ _
nitrobenzcne
__ pentachlorophenol
__ pyridine
__ tetrachloroethylene
__ trichloroethylene
__ 2,4,5-trichlorophenol _____ _
__ 2,4,6-trichlorophenol _____ _
__ vinyl chloride
endrin
lindane
__ methoxychlor
__ toxaphene
2,4-0
_ 2,4,5-TP (Silvex)
I N.C. Department of Environment,
1 lcnlth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wi!rning10n S!r:.~l
Raleigh, North Carolina 27611
le,ite Number__,_/l,Jl.1/4--='C£}:J,=--"'{l--".6'-. ,._=-'~5:',""'3'"""-"._s-"--_--,,_/_,_?_·.._7-'Field Sample ,Number_~/)~/_7 _ _.'?~0~7~-----
Name of Site_--"lj_:S'-"'-,.,; '4: .,,IJ,-.1ccft,.,n'-'-... .)/"""'""1-L)"-'/;C-L_-.._{ ___ Site i,;,cation _________________ _
Collected By ~ 5 t{2,A/1~/ ID# ___ Date Collected_tL/-_:7-:_ __ q,,_,-l-a.L~_L,_ __ Time _____ _
/~d TCLP Compounds
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Agency: Hazardous Waste
Sample Type
Environmental
Ground water (1)
Surface water (2)
_Soil (3)
_ Other (4)
Concentrate
Solid (5)
Organic Chemistry
Parameter
P&T:GC/MS
Aeid:B/N Ext.
MTBE
Results(mg/1)
•-----l
Solid Waste
Inorganic Chemistry
Parameter Results(mg/1) (mg/kg)
__ Arsenic ",fe: fl.., oH Vr,I,',,
B . ,¥• t __ anum O />rl.., i.,,, Io
__ · Cadm_ium S_;, "'i' (, 1 ( C; ~ i,l.
__ Chlonde .A)o.,;, 1 ·7: :r o ,:+ U JI I
__ Chromium ~eC(94t @1.'t 1:4
__ Copper p /4 :,;± TL,. i:i "'""
_ Fluonde -~f: ~"",.j_ '."'"'eJ.-; .· _ Iron (?.. S q.,t:. 9. 4/ -;. ,, t . t
_·_ Lead Th ., h ...,e a
_·_·· Manganese c.,, if ~,-,fiQu,
__ Mercury
Nitrate
Selenium
Silver
Radiochemistry Sulfates I ,_P_a_r_a_m_e-te_r __________ __,_~P~.
Results (PCi/1) ...JL'PH . 4, • :'3
I __ Gross Alpha __ Conductivity
Gross Beta TDS
TOC
I Microbiology
1-------l
I
I
Parameter Results (Col/1001111)
Date Received _________ Reported by _________ _
Dale Extracted Dated'" ort~ 0 -------Or~.~ "."1. SEP 2 ';7
Dale AnalyLcd Lab Number
n11<.: ,101 111~,,;,..-a-,-,,-,,-, ------------------
Inorganic Compounds
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-eresol
m-cresol
__ p-cresol
cresol
1,4-dichlorobenzene
1,2-dichloroethane
Results(mg/1)
Results(mg/1)
-------
-------
__ 1,1-dichloroethylene ______ _
2,4-dinitrotoluene _
__ heptachlor
hexachlorobenzene
hexachlorobutadiene
hexaehloroethane
methyl ethyl ketone
nitrobenzene
__ pentachlorophenol
__ pyridine
tetrachloroethylene
__ trichloroethylene
__ 2,4,5-triehlorophenol
__ 2,4,6-trichlorophenol
__ vinyl chloride
endrin
lindane
methoxychlor
toxaphene
2,4-0
__ 2,4,5-TP (Si!·,ex)
-------
-------
I
' '
N.C. Department of Environment,
1 lca!Lh, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
le,ile Number /l/C:/) 0@2. SSS-7o/'z Field Sample Number
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Name of Sile ~i11en t,ftr Site i;,cation
Collected By ; 5 tan£; rn# Dale Collected
Agency: Hazardous Waste Solid Waste /~fund
Sample Type
Environmental Concentrate Comments
__ Ground water (1)
__ Surface water (2)
_Soil (3)
Solid (5)
Liquid ( 6 ~ ~'..:..!::.~C:,c.J&J"-'1 &cf'.".!,1,,~Ji,t,.:U<,:1'.,_jt""®'....:'./,,:.;,(/c!.m.<.!
Sludge (7) ~~~~'-"-''--'r-¼~· "'. ,,_ __ _
_ Other (4)
Organic Chemistry Inorganic Chemistry
Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg)
_P&T:GC/MS Arsenic
Acid:B/N Ext. Barium
MTBE Cadmium
Chloride
Chromium
__ Copper
Fluoride
Iron
Lead
__ Manganese
__ Mercury
Nitrate
Selenium
Silver
Radiochemistry Sulfates
~ Parameter Results (PCi/1) ~ .. .(_I
__ Gross Alpha __ Conductivity
Gross Beta TDS
T0C
I Microbiology
1-------l
Parameter Results (Col/lOOml)
I Date Received Reported by
I Dale Exlraclc<l D?_le ~_e_pQI\\;d 2~7 ut.,:,<' ,· L SEP
Dale Analyzed Lab Number
State Laboratory of Public Health
P.O. 0ox 23047, 306 N. Wilmington St:-:.~l
Raleigh, North Carolina 27611
D/7 3u3
TCLP Compounds
Inorganic Compounds
Arsenic
Barium ,
Cadmium
Chromium
Lead
__ Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
ch!orobenzene
chloroform
o-cresol
m-cresol
p-cresol
cresol
Results(mg/1)
Results(mg/1)
-------
1,4-dichlorobenzene ______ _
1,2-dichloroethane
__ 1,1-dichloroethylene ______ _
2,4-dinitrotoluene.
__ heptachlor
hexachlorobenzene
hexachlorobutadiene
hexachloroelhane -------
methyl ethyl ketone ______ _
nitrobenzene
__ pentachlorophenol
pyridine
__ tetrachloroethylene
__ trichloroethyle□ e
__ 2,4,5-trichlorophenol ______ _
__ 2,4,6-trichlorophenol ______ _
__ · ,inyl chloride
endrin
lindane
melhoxychlor
__ toxaphene
2,4-D
__ 2,4,5-TP (Si!·,cx)
I '
I N.C. Department of Environment,
. I !cal th, & Natural Resources
Solid Waste Management DiVlsion
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Dax 2.3047, 306 N. Wilmington Str=.ct
Raleigh, North Carolina 27611
... ite Number· /;/C.£} O(J;, 2-,2SS-79'7 Field Sample,Number _ __.0"'--'-/_7.,__~3'-"'0'---"Y=!-------
~l):1dn ~ <{;L)fr ( Site u:ication ____ ~~-------I Name of Site ?) Tuf'/TJ; ID# ____ Date Collected_.iL,'-=--'---1---/,,L~-'---Tirne _____ _
Hazardous Waste Solid Waste ~nd TCLP Compounds
Collected By
I
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I
I
Agency:
Sample Type
Environmental
__ Ground water (1)
__ Surface water (2)
Soil (3)
Concentrate
_ Solid (5)
_ Liquid (6 ,2t''-?tt!C [{f1,,J&trbm
_ Sludge (7) Q/J f} l:i,~#li)
_ Other (4) _ Other (8) 3 -tY!, -(JI,(! 11/rv!J= ZD3Q C •~--~--/! ---
I
I
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I
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I
Organic Chemistry -Inorganic Chemistry
Parameter
P&T:GC/MS
Acid:B/N Ext.
MTBE
Results(mg/1) Parameter Results(mg/l)(mg/kg)
Radiochemistry
Parameter Results (PCi/1)
__ Gross Alpha ______ _
Gross Beta
Arsenic
Barium
Cadmium
Chloride
Chromium
__ Copper
Fluoride
Iron
Lead
__ . Manganese
__ Mercury
Nitrate
Selenium
Silver
Sulfates
~-
--Conductivity ______ _
TDS
TOC
I Microbiology ~---
I
I
Parameter Results (Col/lOOml)
Date Received _________ Reported by _________ _
Date Extracted Date Reported ------u•·'.·;·.c:,,,-s-E-f)-•-,,-~,----.J._:~.1... I ... ..) L I
Dale AnalyLed Lab Number
Inorganic Compounds
Arsenic
Barium ,
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
rn-cresol
__ p-cresol
cresol
1,4-dichlorobenzene
1,2-dichloroethane
Results(mg/1)
Results (mg/I)
-------
-------
__ 1,1-dichloroethylene ______ _
2,4-dinitrotoluene.
__ heptachlor
hexachlorobenzene
hexachlorobutadiene
hexachloroethane
methyl ethyl ketone
nitrobenzene
__ pentachlorophenol
__ pjTidine
__ tetrachloroethylene
__ trichloroethylene
-----~-
-------
__ 2,4,5-trichlorophenol ______ _
__ 2,4,6-trichlorophenol ______ _
vinyl chloride
endrin
lindane
methoxychlor
toxaphene
2,4-D
__ 2,4,5-TP (Si!·1cx)
I
I '
N.C. Department of Environment,
1 lc.:ilth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. 13ox 2SO-l7, 306 N. Wilmington Stn:~l
Raleigh, North Carolina 27611
~ile Number /;/Cd) 06 Z. ,2SS-7r·z Field Sample ,Number_--1a6..,_./'--,-'-3~0~.;-______ _
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--2uJ IJ1 Qn ~fr -{ Site 'Glcation ____ ---,---________ _ --? ) tanlf ID# ____ Date Collected_,L.Jc.:::...--'-_;_-L--'----Time _____ _
Name of.Site
Collected By
Agency: Hazardous Waste Solid Waste ~d TCLP Compounds
Sample Type
Environmental Concentrate
__ Ground water (1) _ Solid (5)
Surface water (2) _ Liquid (6
_Soil (3) _ Sludge (7)
_ Other (4)
Organic Chemistry Inorganic Chemistry
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg)
P&T:GC/MS Arsenic
Acid:B/N Ext. Barium
MTBE Cadmium
Chloride
Chromium
Copper
Fluoride
Iroo
Lead
__ . Manganese
__ Mercury
Nitrate
Selenium
Silver
Radiochemistry Sulfates
~ Parameter Results (PCi/1) ~~7
__ Gross Alpha __ Conductivity
Gross Beta TDS
TOC
Inorganic Compounds
Arsenic
Barium ,
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
__ p-cresol
cresol
1,4-dichlorobenzcne
1,2-dichloroethane
1, 1-dichloroethylene
--2,4-dinitrotoluene.
__ heptachlor
hexachlorobenzene
hexachlorobutadicne
hcxachlorne_thane
methyl ethyl ketone
nitrobenzene
Results(mg/1)
Results (mg/I)
-------
------~
-------
-----~-
I Microbiology
t-----------1
__ penlachlorophenol
pyridine
tetrachloroethylene
__ trichloroethylene
I
I
Parameter Results (Col/lO0ml)
Date Received Reported by --------------------
Dale Extracted Date ~,Qo,n.e~.,,. -------u .J..,:-:" 7,' ....... -il...,S'"'Ea,r, .... -L.,_, "9""'7--
□stc Analyzed Lab Number
__ 2,4,5-trichlorophenol ______ _
__ 2,4,6-trichlorophenol
vinyl chloride
endrin
lindane
methoxychlor
toxaphene
2,4-D
__ 2,4,5-TP (Si!·,cx)
-------
I
I •
N.C. Department of Environment,
1 lca!th, & Natural Resources
Solid Waste Management Division
SA.i\1PLE ANALYSIS REQUEST State Laboratory of Public Hc:i.hh
P.O. I3ox 280-17, 306 N. Wilmington Street
Raleigh, North Carolina 27611
~ ite N umber--1./t_,,_/,_,,C:::,-:/""--)-"a"'>i:i'--. =-=2.=-.., 5::'<C,:5".L.,.s-,<___---?._,_/_,?c_',,:;2_cFicld Sam pie ,N umber _ __.(J-"-!_1~.J~u_._u~· ------
~ /l })1{1n ~t (< Site i;,cation ____ ---,-________ _ 1 . Name of Site
Collected By
I Agency:
~) tuf'/4 ID# ___ Date CoUected_lL./---=----'--+-.,___,_ __ Time _____ _
~nd TCLP Compounds
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I
Hazardous Waste Solid Waste
Sample Type
Environmental Concentrate
_ Solid (5) __ Ground water (1)
Surface water (2) Liquid (6 1l&m
_ Soil (3)
_ Other (4)
_ Sludge (7
_ Other (8)
1~--~-----,
Organic Chemistry Inorganic Chemistry
I Parameter Results(mg/1) Parameter Resulls(mg/l)(mg/kg)
I
I
_· P&T:GC/MS
Acid:B/N Ext.
MTBE
Arsenic
Barium
Cadmium
Chloride
Chromium
__ Copper
Fluoride
Iron
Lead
Manganese
__ Mercury
•t--------i
Nitrate
Selenium
Silver
Sulfates I Radiochemistry
Parameter Results (PCi/1)
__ Gross Alpha I Gross Beta -------
~ __ Conductivity
TDS
TOC
I Microbiology 1------i
Parameter Results (Col/lO0ml)
I Date Received Reported by
Date ExtrnctcJ Date Reported
I 01,--,,,. ~~i.. t' ,:_;
Date Analyzed Lab Number
n' .,. ~ •,. • '"
SEP 297
Inorganic Com pounds
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
__ p-cresol
cresol
1,4-dichlorobcnzene
1,2-dichloroethane
1, 1-dichloroethylene
2,4-dinitrotoluene.
__ heptachlor
hexachlorobenzene
hexachlorobutadiene
hexachloroethane
methyl ethyl ketone
nitrobenzene
__ pentachlorophenol
__ pyridine
tetrachloroethylcne
__ trichloroethylenc
Results(mg/1)
Results (mg/I)
-------
-------
-------
-------
__ 2,4,5-trichlorophenol ______ _
__ 2,4,6-trichlorophenol ______ _
__ vinyl chloride
endrin
lindane
methoxychlor
toxaphene
__ 2,4-D
__ 2,4,5-TP (Sil·,cx)
I
I '
N.C. Department of Environment,
! [callh, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Hc:alth
P.O. Dax 28047, 306 N. Wilmington Strccl
Raleigh, North Carolina 27611
.. i:: ~umber /VC.£} 0@ 2.. ,2SS-7f'7 Field Sample ,Number_--'(2-"--'/'--'J'------")'-G::::.'------,7f------
__Sll /}1 ffi1 ~t { Site ~cation ____ ~---------Name of Site ~_) taY/!dy ID# ___ Date Collected :?j~::-_-'.:..._q,+l_f_1_"_J ___ T_im_e==========-~
Hazardous Waste Solid Waste [~nd TCLP Compounds
I Collected By
I
I
I
Agency:
Sample Type
Environmental Concentrate
Ground water (1) __ Solid (5)
• _ Soil (3)
_·_Other (4) -Other (8)
I
I
Organic Chemistry Inorganic Chemistry
Parameter
_-P&T:GC/MS
Acid:B/N Ext.
MTBE
Results_(mg/1) Parameter Results(mg/l)(mg/kg)
Arsenic
Barium
Cadmium
Chloride
Chromium
__ Copper
Fluoride
Iron
Lead
__ ·Manganese
Mercury
Nitrate
Selenium
Silver
0 Radiochemistry Sulfates
,--------'-~pHi
n
Parameter .Results (PCi/1) _JL:'.'P_H _
_. _._.Gross Alpha __ Conductivity
Gross Beta TDS
TOC
D 1----rv_r_ic_r_o_b_io_l_o_gy ____ --l
Parameter Results (Col/JOOml)
D Date Received _________ Reported by _________ _
Date Extracted _________ Date R.<p->1r~A-~..._,,,,_ ~,:~· ______ _
Ul,,t.,, _, SEP 297
Date Analyzed Lab Number
Inorganic Compounds
Arsenic
Barium ,
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
p-cresol
cresol
1,4-dichlorobenzene
1,2-dichloroethane
Results(mg/1)
Results(mg/1)
-------
-------
1,1-dichloroethylene ______ _
2,4-dinitrotoluene _
heptachlor
hexachlorobenzene
hexachlorobutadiene
hexachloroethane
methyl ethyl ketone
nitrobenzene
__ pentachlorophenol
pyridine
__ tetrachloroethylene
__ trichloroethylene
__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol
__ vinyl chloride
endrin
lindane
methoxych!or
toxaphene
2,4-D
__ 2,4,5-TP (Sibcx)
-------
I N.C. Department of Environment, SAMPLE ANALYSIS REQUEST State Laboratory of Public Hcalth
! [cal th, & Natural Resources P.O. 0ox 28047, 306 N. Wilmington Stn:.:t
Solid Waste Management Division Raleigh, North Carolina 2761 l
..,ite Number /l/ C.£) 06 2-5S s-7rz Field Sample ,Number_....,,Oe:._,/,___J~>~D~· ~i~_· _·· -----
I
I
I
I
I
Name of Site ~iyJ!o/n ~f { Site i,;,cation _____ ~------------
Collected By 7) fr2t17+ ID# ___ Date Collected X/4~,(-_-:.._(,_,lc....}_t_J_---Z ____ T_i_m_e:==========~
Agency: Hazardous Waste Solid Waste /~nd TCLP Compounds
Sample Type
Environmental
__ Ground water (1)
__ Surface water (2)
_ Soil (3)
Concentrate
_ Solid (5)
_Llq~d0~~~=~~~=~=~~=
_ Sludge (7) ~/l.~"~· ~~,~:='2,..·~.c.+----
Inorganic Compounds
Arsenic
Barium
Cadmium
Chromium
Lead
__ Mercury
Selenium
Silver
Results(mg/1)
... -Other (4) -Other (8) .55:-. ;z~tw lsJVB ;zo31 l1 I ~---~-1-------;
Organic Chemistry Inorganic Chemistry
I Parameter Results(mg/1) Parameter Result.s(mg/1) (mg/kg)
_P&T:GC/MS Arsenic
Acid:B/N Ext. Barium
MTBE Cadmium
Chloride
I Chromium
__ Copper
Fluoride
Iron
I Lead
__ . Manganese
__ Mercury
I Nitrate
Selenium
Silver
I Radiochemistry Sulfates
~ Parameter Result.s (PCi/1) L;..,~
I __ Gross Alpha __ Conductivity
Gross Beta TDS
TOC
I Microbiology
1------1
Parameter Results (Col/lOOml)
I Date Received Reported by
I Dale Extraclc<l Date QlPft7d;···
h,L I f SEP 297
Dale Analyzed Lab Number
'" ,,. """ ,,,
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
__ p-cresol
cresol
1,4-dichlorobenzcne
1,2-dichloroethane
1, 1-dichloroethylene
2,4-dinitrotoluenc.
__ heptachlor
hexachlorobenzene
hexachlorobutadiene
hexachloroethane
methyl ethyl ketone
nitrobenzene
__ pentachlorophenol
p)Ti<line
__ tetrachloroethylene
trichloroethylene
Results(mg/1)
-------
-------
-------
-------
-------
__ 2,4,5-trichlorophenol ______ _
__ 2,4,6-trichlorophenol ______ _
__ vinyl chloride
endrin
lindane
methoxychlor
__ toxaphene
2,4-0
__ 2,4,5-TP (Sil·1cx)
I N.C. Department of Environment,
I !calth, & Natural Resources
Solid Waste Management Di..,ision
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina •27611
a.site Number /;/Cf} 0@2.. ,2SS-7f'•z Field Sample,Number _ __._[)c...J__/_7'--""'3'-0c.......,9<-------
Narne of Site_~_S""'-,...; "4 . .,.ly!µ,.io/n.i.,_;.__,'= ~.,,,'./Jl-Lt'---'-_-.,_( ___ Site ~cation _____ ~------------
Collected By 7, 5 tuf1~ ID# ___ Date Collected XP-(, /q --z Time ____ _
Hazardous Waste Solid Waste ~d TCLP Compounds
I
I
I
I
I
Agency:
Sample Type
Envirorimental
Ground water (1)
Surface water (2)
_ Soil (3)
··_··_Other (4)
Concentrate
_ Solid (5)
_ Liquid (6 t(h4r:L4m
Sludge(7) /J/} ,?QY..J
_ Other (8) 55-3?-l'tJ / BrJ/t 20 3 / 7
) 1-------~
Organic Chemistry Inorganic Chemistry
I
I
I
Parameter
P&T:GC/MS
Acid:B/N Ext.
MTBE
Results (mg/I) Parameter
Arsenic
Barium
Cadmium
Chloride
Chromium
__ Copper
Fluoride
Iron
Lead
Results (mg/I) (mg/kg)
•f.----l
__ Manganese
__ Mercury
Nitrate
Selenium
Silver
Radiochemistry Sulfates 11-----------'----l_~pZHi
Parameter Results (PCi/1) _J.L'.'"PH . Z, (9,
__ Gross Alpha _________ Conducti,ity ______ _
I Gross Beta TDS
TOC
I Microbiology
II--~-'--
P:..irameter Results (Col/1001111)
1 · Date Received _________ Reported by _________ _
Dale Extracted _________ Dale Reported I Dale AnalyLed Lab NumbQJ'.:',--:-2_7_•s_.:_s_E_P __ 2_9_7_
Inorganic Com pounds
Arsenic
Barium ,
Cadmium
Chromium
Lead
__ Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
__ p-cresol
cresol
1,4-dichlorobenzene
1,2-dichloroethane
Results(mg/1)
Results(mg/1)
------~
-------
1,1-dichloroethylene ______ _
2,4-dinitrotoluenc _
__ heptachlor
hexachlorobenzene
hexachlorobutadiene
hexachloroelhane -------
__ methyl ethyl ketone ______ _
nitrobenzene
__ pentachlorophenol
__ pyridine
tetra chloroe th yl en e
__ trichloroethylene
__ 2,4,5-trichlorophenol ______ _
__ 2,4,6-trichlorophenol ______ _
__ ,inyl chloride
endrin
lindane
_· _ methoxychlor
__ toxaphene
__ 2,4-0
__ 2,4,5-TP (Sil·,cx)
I
4·
N.C. Department of En-.ironmcnt,
I lcillth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
-..,ilc Number /l/Cf) 06 2 SSS-7?7
~,non i1(1fr r
Field Sample ,Number
I
I
I
I
I
I
I
I
.I
' Name of Site Site Location
Collected By ; 5 ta11!~/ JD# Dale Collected
~fund Agency: Hazardous Waste Solid Waste
Sample Type
Environmental Concentrate
_ Solid (5) __ Ground water (1)
Surface water (2)
_ Soil (3)
11
Liquid (6 ·t@n-i
Sludge (7) ="--LL--"''-"'-''-'--'-""-.,_ __ _
_,_., Other (4) Other (8)
Organic Chemistry
Parameter
P&T:GC/MS
Acid:B/N Ext.
MTBE
Results(mg/1)
--------·------
f---------------~
Inorganic Chemistry
Parameter
Arsenic
Barium
Cadmium
Chloride
Chromium
__ Copper
Fluoride
Iron
Lead
Results (mg/l)(mg/kg)
__ Manganese
__ Mercury
Nitrate
Selenium
Silver
I Radiochemistry Sulfates
1--------'~ -~pH;
Parameter Results (PCi/1) ..µc'.'.'.'PH . I~ . 5
__ Gross Alpha _______ __ Conductivity ______ _
Gross Beta TDS
TOC I
I Microbiology
1------J
I
I
Parameter Results (Col/lO0ml)
Date Received _________ Reported by _________ _
Date Extracted _________ Date Reported
01~:.:··=73~. -S-EP_2_9~7--
Lab Number Dale Analyzed
nIr<.: i.1111rD,.,.:~ .. c111u1\
Scrn: l....aboratory of Public Hc;;lth
P.O. Oox '.!S0-47, 306 N. Wilmington Str=ct
Raleigh, North Carolina 27611
TCLP Compounds
Inorganic Compounds
Arsenic
Barium ,
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
'
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresol
__ p-cresol
cresol
1,4-diehlorobenzene
1,2-dichloroethane
1, 1-dichloroethylene
2,4-dinitrotoluene.
__ heptachlor
hexachl'cirobenzene
hexachlorobutadiene
hexachloroelhane
Results(mg/1)
Results (mg/I)
-------
-------
-------
-------
__ methyl ethyl ketone ______ _
nitrobenzene
pentachlorophenol
p)Tidine
__ telraehloroethylene
__ trichloroethylene
__ 2,4,5-triehlorophenol --'------
__ 2,4,6-trichJorophenol ______ _
__ vinyl chloride
endrin
lindane
__ melhoxychlor
__ toxaphene
2,4-D
__ 2,4,5-TP (Si!·1cx)
I
t I •. 41
N.C. Department of Environment,
I !calth, & Natural Resources
Solid Waste Management Di,.ision
SA.t\1PLE A.t'\'ALYSIS REQUEST State Laboratory of Public HcJlth
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
..,ile Number /;/Cf) C& 2 ,2SS-7'1'7 Field Sample ,Number _ ___.:D~/_7-'-,2~2~/...,J~------
I Name of Site ~ )J1fTn ,)//)t-f Site u'.ication ____________ _ ? ) j-{l,'(lw; ID# ____ Dale Collecled_.u,1---=-__:---1--_,__.L.... __ Time _____ _ Collected By
I Agency: Hazardous Waste " Solid Waste /~nd
I Sample Type
Environmental Concentrate
_ Solid (5)
_ Liquid (6',\\.e~~~:.k'.~t..e,ttC!.',Jt~l,,_c,"'l"-o~/~"'il-1'1=
_ Soil (3) _ Sludge (7) Q/J f} D,;/llt) · ·
_,,,/
I Ground water (1)
__ Surface water (2)
I
-Other (4) -Other (8) 5S'hJD f5 l!ltl/} Zo·5 zD I ~--------1 __ _____,
Organic Chemistry Inorganic Chemistry
I Parameter Results(mg/1) Parameter Results (mg/l)(mg/kg)
P&T:GC/MS Arsenic
Acid:B/N Ext. Barium
MTBE Cadmium
Chloride
I Chromium
Copper
Fluoride
Iron
I Lead
Manganese
__ Mercury
I Nitrate
Selenium
Silver
I Radiochemistry Sulfates
~ Parnmett:r Results (PCi/1) [<;_ :z
I __ Gross Alpha __ Conductivity
Gross Beta TDS
TOC --
I Microbiology
1----------1
I
I
Parameter Results (Col/l00ml)
Date Received _________ Reported by _________ _
Date Extracted _________ Dale Reported ________ _
Dale Analyzed
l·,·1· ~--,,.,..., <:,i:cLF' ?"77 J,_f-..l.. •.•. ) --
Lab Number
TCLP Compounds·
Inorganic Compounds
Arsenic
Barium
Cadmium
Chromium
Lead
?-.fercury
.Selenium.
Silver
Organic Compounds
benzene
carbon tetrachloride
chlordane
chlorobenzene
chloroform
o-cresol
m-cresoI
p-cresol
cresol
1,4-dichlorobenzcne
1,2-diehloroethane
1, 1-dichloroethylene
2,4-dinitrotoluene.
__ heptaehlor
hexachlor6benzene
hexachlorobutadiene
hexaehlornethane
methyl ethyl ketone
nitrobenzene
__ pentachlorophenol
p)Tidine
tetrachloroethylcne
__ triehloroethylene
__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol
__ . ,inyl chloride
endrin
lindane
methoxychlnr
toxaphene·
2,4-D
2,4,5-TP (Si!·,cx)
Results(mg/1)
Results(mg/1)
-------
----~--
I. N.C. Department of Environment,
I lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
.. e Number NCO Or:;; 2--S-SS 7C/ Z... Field Sample Number Of 7 '?:£) (
Name of Site SJ3rno/l .S 5.t'-f-h 'c... 72<,;t /c._ Site Location Sf deJ VI / /e__ I Collected By l)w ID# ___ Date Collected -?:i/2-0 I t?1 Time D1{ 0
I Agency: Hazardous Waste Solid Waste Vs u per fund TCLP Compounds ----
Sample Type Ino11:anic Compounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
S/0c(q--: St;'!f /e Barium --
__ Groundwater (1) _ Solid (5) --Cadmium,
I Chromium
_·_ Surface water (2) loe,OOC'\. '/i-'S --
_ Liquid (6) Lead ---J
tE'e+ __ Mercury
I _ Soil (3) V Sludge (7) t>eq1~ (o-l\ Selenium --Silver
_ Other (4) _ Other (8) ss--;,s.-\AJ s --
--
--I --
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Resul:1 ( mtlj (ng/kg) Organic Compounds Results(mg/1)
_ P&T:GC/MS -b;-Arsenic L.... 5 "c-1 benzene --
-Acid:B/N Ext. Barium ;J..5o carbon tetrachloride
-C Cadmium --
MTBE z..9. g chlordane ------Chloride chlorobenzene ------
(_,,. Chromium ~8D chloroform ----
·I --_._Copper o-cresol --
• P, .. Fluoride m-cresol ------
Iron p-cresol ------
I --~ Lead z,,g cresol --
--__.L. Manganese \1n 1,4-dichlorobenzene --
--L,,-Mercury .. 0, 2r, --1,2-dichloroethane
Nitrate __ 1,1-dichloroethylene --I --L, Selenium L_;;J.. 2,4-dinitrotoluene --V Silver ""-9 .p, heptachlor ----
Radiochemistry Sulfates hexachlorobenzene
I ----
······-·· Zinc hexachlorobutadiene
Parameter Results (PCi/1) ----hexachloroethane --pH --
__ Gross Alpha --Conductivity · __ methyl ethyl .ketone
I --Gross Beta TDS nitrobenzenc --TOC __ pentaehlorophenol. --__ pyridine --
I Microbiology --tetrachloroethylene --
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5:tri~hlorophenol --__ 2,4,6-trichlorophenol ----__ vinyl chloride ----endrin --lindane --I Date Received Reported by __ methoxychlor
... __ toxaphene
Dale Exlraclc<l Dale Rc't'J1e~18 2,4-D
., •..
I
--0 AUG2697 _ 2,4,5-TP (Silvex)
Dale Analy,e<l Lab Number --
!)JlS l\!Jl (llcviscd 2/91)
,, ' j
t\ • ~ :.
I N.C. Department of Environment,
· I lc3hh, ·&· N:ilural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory o( Public Health
P.O. Box 280:t7, 306 N. Wilmington Street
Raleigh, North Carolina 27611
lie Number Alco Cro z__ sss 712.... Field Sample Number CQ (] ·z...sc;
Name of Site St3rno/1 .5 'Sq?ii 'c... 7g;t /c.. Site Location S,f q}ey VI //e_
I Collected By J S ID# ___ Date Collected 'B( 21,,( 17 Time / <f-::,D
I Agency: Hazardous Waste Solid Waste Vsuperfund TCLP Compounds
----
Sample Type Inorganic Com pounds Results(mg/1)
I Environmental Concentrate Comments Arsenic --
~i cfalfh, LJ/e l(
Barium
V Ground water (1)
--
Solid (5) Cadmium --Chromium' 1--Surface water (2) SS-o/-Pw --
_ Liquid (6) Lead --
+tfJ /V fC-1 NCy
__ Mercury
_ Soil (3) _ Sludge (7) Selenium
I Other (4)
--
v.JGL,L-i-
Silver
UJAf'E(2-.. --
Other (8) --
SS-ol-Plv --
I --
Organic Chemistry Inorganic Chemistry --
I Parameter Results(mg/1) Parameter Results(mg/l)t RIil Ill Organic Compounds Results(mg/1)
--P&T:GC/MS (/ Arsenic < 0, (2 / benzene --
Acid:B/N Ext. v Barium <o,; carbon tetrachloride
-----c:" Cadmium --
MTBE S:.:o,oo.r: chlordane ----
Chloride chlorobenzene ----<o. 01
--
--____l:CChromium chloroform --
I
. , ,' .... __ Copper o-cresol ----
--Fluoride m-cresol ----Iron _· _ p-cresol ----
--V Lead &z~:r cresol
I ----
--V Manganese --1, 4-dichlorobennne
V Mercury ..::_,::_ <::-cP5 __ 1,2-dichloroethane --
--V Nitrate __ 1,1-dichloroeth_ylene
I ~ Selenium ~ .o ... GI 2, 4-dinitrotoluene --
-V Silver (o, oS:: __ heptachlor --
~adiochemistry Sulfates hexachlorobenzene ----
I ····----·-Zinc hexachlorobutadiene
Pi.iramelt:r --Results (PCi/1) 1 c tJH hexachloroethane --
__ Gross Alpha --Conductivity __ methyl ethyl ketone
I Gross Beta TDS nitrobenzene ----TOC __ pentachlorophenol --__ · pyridine
I Microbiology ~-re: ,/Ji t .-~ f-.,_ __ tetrachloroethylene
~e,_, t:: ~ l.d "-~ __ trichloroethylene
P;iramcter Results (Col/lOOml) ~to·, r;;_,, ed. Co ..,.ol0 1 __ 2,4,5-trichlorophenol
--r __ 2,4,6-tricWorophenol --
----__ vinyl chloride
endrin --lindane
I Date Received Reported by --
--methoxychlor
toxaphene --
Dale Exlracleu Date Reported 2,4-D
012t_1S AUG 2B '-) I --
I _ 2,4,5-TP (Silvcx)
Dale AnalyLeu Lab Number --
J)I !S Jl'Jl (1\cviscd 2/91)