NCD062555792_19980707_Sigmons Septic Tank Service_FRBCERCLA C_Groundwater Section correspondence 1987 - 1998-OCR

NCD0820:;:;792
Sig,non's Septic
Ta.nk Service
Groundwater Section
correspondence,
19S7-I99S
Julg?,L998
COlfNTY
QUAD NO
IRUH:1.1. S,\.\11'1.I: l'RIURI I Y
~ROUIINE □Er-tER(iUWY
REPORT 10 _>010R010)cccc~~----Re!tif'n.,! ll!licc
COlLEClOR(SI KRf:0S!~lURRIS
~ CHAIN or cus 1 ODY
EJ SAMl'l.E ·1 Yl'E □ u..-. 1 f: 1nr1s
Tl.\lE
PURPOSE
LABORATOI!\' ANALYSIS
BOU JlO "'fl. L
COU lli~h HO "'!t I.
COD low )JS "'fl.I,
Coliform MFhuJ Jlt,it, IIC~J,nl
Coliform MF focal JI 50-! /IOOrnl
roe mtt·l
Twbitiiy NIU
RMiduor. Sulf'('f><kJ 1.10 "'!t L
Total Su~ wliJ, mitl.
'" unin
Allalinity lo rl I 4 S "'ll I.
Aluliniry lo pll I J "'fl. I.
C•bon.iilt tnll I.
Bica-bona!, m11I.
C•bon d,01i<k mlll.
(hlori<k mil I.
Chromium lln 10.1: Ult\.
Color True 110 "'
CuniJc 1:0 "'" I
CO.\l:\IF.."1TS:
(h,nc,
l.,..:n1ion 01 Si1c
JOIIN l.,\MBEH 111 WELi. J
lks.-rir1i"n ,,r ,.,mplin!!-r<'in1 _______________________ _
S.11nplin1t MrthnJ
lfrmn,~•
IJi« SnliJ5 70JOO me:/1. ,\!1-•Siher 465&<,
l-lurniJc QS I "'!UL ,\l•Aluminum 4b55 7
l[;u<l11c11 101nl 900 "'El'\. 1\s•AfSCPliC 4(,551
l l;u<lncu {non-ca,h) ',II)~ "'F-'L 113-llaiium 46558
l'hcnol, )2710 U!t/l. Ca-Calcium 46552
Spn:ific Cond Q5 umho~'em2 Cd·C-adium 46559
Sulf~ie m[i.'L Cr•Chrnmiurn 4(,560
Sulfide H5 m(l'L Cu-Copper 10.12
\lll,\S m(l'L Fe· hon 10~5
Oil 1111d Gmiu mEL1L Ilg• Mercm,· 71900
Silic.11 "'EL'L K-l'ulassium 46555
Bomn Mp:· Maf!ne~ium 927
I oimalddl\ de m1_t.'L Mn-Mang;u,ese 1055
NIIJuN610 mit:l Na-Sodium 929
IKNuN625 mg'L Ni-Nic\..d
NU~ •NO.I un630 mp;'L ' l'b-1.ead J<,S&-1
I' I otal a, I' (.C,5 mp:1L Se-Selenium
l'OJ n•~·L 7.n Zinc -l'J567
ug:l.
ug,L
ug/1.
ug/1.
rng/1.
o!'/L
u11,IL
ug/L
ug/L
op/L
mg/L
rng/1.
ug/1.
rng/L
ug/L
<10ug/L
u[l}l.
ug•L
I imc f-lcrci,cd
lfrcci.ed lh
Rde~scd th IJS
ll.11e rqw,tc,I · Q/101911
O,i,: .. uuchluri"c l'nlicidcs
Ocg:rnophosphorus f'estic;dcs
Ni1,ngcr1 l'esiicidn
Acid llcibieidcs
Scmi,olatilcs
11'1 l•Dicsc! Rru,ge
Volatile Organics t \"(),\ l,oitle)
I l'l l•Gasolir1c Ran1-cc
I l'l l•ll [ E:< Gasoli,1c Range
er.1'1f'>6JVl
Nor 111 Caroll11a
G OUNDWATER FIELD/LAB FORM Dcpnr lmenl of E11vl,01111w11!, 1 lenllh, and Nalur :ii ncsowce!'l
DIVISION OF WATER OU/\LllY -GllOUNlJW/\TEfl SECTION •
--I,e_l'=-Ofiu_ eMPLE TYPJ: SA~1~L~ p111Qnifv_:
L "--l'l3 Serial No._______ ~Water Enoullne
0
,: .. ·· .
-' n D Soll D E111erc•ency
Lal. 3S-·· 'I 1-C,(p I n,) -<;S • O'Z.. LJ~~==="'========c'~===~ · 1
.onu. -="-----~'-'-'-"--='--Olher __________ _
neporl To: 11no, rn~mo. Wano, WillO, ~Chain of Cuslody
WSRO, Klnslon ro. red. Trusl, Cenlrnl 011., Olher: __________ _
IJ;ila E11hy Uy.: ________ Cir: ____ _
I.Jale f1epor led: ______ _
Shipped by: ()us, Courie land Del. Oilier_· _____________ _ P111posn:
Colleclor(s}: K~c:U f\10lt.1J Dale ..l/.l(..1.. .• 1~;, ___ Time ~o~ci~, o~---Bc1:,r.li11~0111pli;111cf',,I.U~) I'. Pr.slicidn Slt1dy, Fndt!rat I fllSI, U!11m: ------
FIELD ANALYSES owner :forl"--\ ~.c·H._____,,,w"-'--''"_c1.,,,,,,.;:__~'"'_""_'' ______________ _
pll,
00
_____ Spec. Coml.
91
_S-_5 __ al 25° C Localion or sile I 5 2. Lil f'1/Jl.:fl.1L.s~,._ 0--, ".Jr;-, ili'IJOL{,,;___}J,.<..., ___ -Z.=.fs,J,c<±£e...·~_,_._l_
Temp.'° I 0c Odor _ _,_f.J=,)c.f=.J-=~'---Descriplion ol sampling poinl _H.o~~ L-.,!,~ AT bt!.'-f-. ',f h~•~Les:*=~---------
Appenr mice (.JJ:.tv"_ Snr11pli11u Melli ml ____ (2.Ll ,'11\p wi .. ,•,,. toii:r;;;-:-oi;:·,~--------S;1111pl1! l11te,v;il_...1.I.:.< '->--'""'--""":J'------
rield Analysis lly: _______ k_/ll:'.l'.',\ llernar ks--------------~--~~~~-~----------------
LAOOR/\TOR Y AN/IL vsr=s r'f~-Jt,~,\,J"l) t,:,,-\>1 l:!..u_Q'] ''""'''"~"""-·'''''""'' "'"'
_ I IOI 'i. _ :J 1,0 _____ , ________ ---·-! t '!.Ji~
cou.1 lioli :J.I() IH!JII
cor) l.o_~·~-~·~1~ ___ _ ___________ ~ '!!J~I
Coll1011n: t.ff 1"1)Ci!I 111ilfi /11H)rnl
Cold or 111: l.1F I nl;1I :I 1!,!J I
IOCGl\tl
/ 11Hlrnl
llcsidtw, S11::.p1ind1•d !i:111 !Ill/ii -------... --------
--1-----------·----·-------(
/\lk,1li11ily to pl I 11_.:l ,I 1~ _____ I_11qll
111!!'!
__ _ nir.arhrn1;Jlf! ,1-111 _____________ llltj.11
__ C~!_>~!!_1~_l~~~i1~r! __ :,~!:~---____ . ____ r11f!'I
Chloride 9.10 ___________ !~1-~J!I
Chrorni1n11: I lex Ht:l? ~\11_1_
Color: l11w BU CIJ -------------,-
Cyanide /?O rnqll
Lah Co111111e11ts:
lliss._~iulids~·01"o~J'~'"~ _____ rr1utJ_ __
Flour idc 951 1 n!J!~.
l_lardncss: ·r ulal !JOO rnu!!.
I_ l;udrrnss_(11on-car1Jj 90?. l!l!JII_
flltenuls J?.1:JO tiu!! ..
s,wcil!f:. f~_W!d _!)~ l!l:\l!Q::./c;r!I'
'.;1111:1lr! !H!i 111q/l
r!!U(!.
OIi and Grease
!-11\ __ cls_t·J 6H ~,___J ______ _________,lll!JI!
11111 as.l-LG2o rnull.
tJO~_ , _ _t·JO, as_l·J 630 rr)nl[
I': I ota1 as P 6G5 ll)!J1.
___ /\CJ -SilVl!f_•ccJG,0~i_0GG0 ______ ~tl[J/.!
-~!__:_~~l_!~l!!!~ !! (~10 G~oco_l ______ 0UU(!
_ /\s -/\r se 11ic ,I ,G"-5,,_5,___J ---------"ti! 1(!
__ ___!1~~Ll_~i~11 .. 11r._ ·01:Ge,5c,-5::,llc.._ _____ ...-"U!J~(
Cn -Calciw11_,10G'.~i!~l2~. _____ !!!\Ill
"! j/1
~~-~(_!j}l_J~•)ti'.i(i2 (J\)/1
_!_:_e_:_l!_<_!~!__~~~-'-;_:, ________ ...c't\)I~
-~~U--Mercu1y 71_9_1l.<_J ______ u~il_
I( -l'olassiur11 ,Hl5'.J5 111JJ!I
_MU· f·Jlaur1csiu1 011_,\~G~''c'_'l _____ <cll!JII
_r,111 · M;Hlf.JiHH!SC •IG:iG5 __ ..!_!U~!
f J;i -~(JditJHI •1fi'.i~G _ ~!lU/1
-::-7' _l·!i~Jlictc' -(Jy/1
~ _!J!_:_Lr:_;!~ :1.~1.:~r;-1 uu11
Se -Sele11iu111 UU~I
Zn -Zinc •IGJG/
UitJiltl<n:!1lc)1i1HJ l 1!i:;1i<:i<l1!:; --~
{ )qJt1nopltn!;phnr_11s _Pw;licid(JS _
1-lilr_otwn r'(!:;lic:it_lr,J_s_· _____ _
/\ci, I I lei I 1ici( It:'.; ---------------·--·· -----
Vr1l:1tilri ( lr!Ftt1it:'.; __ (y_<Y'':_~~l~~J __ _
! l_'H_:_g,_1:;ol!11~J.l.:_11~u,c __ _
_II~~ I_: !HI: X c~a:_;1~)~n'. !!~'!W!_
,·ot.'NTY
')l'A(lt,:0
IRUlf:1.1.
' " .:: ,· :·, \_
IJl\"ISIOi'\i OF W,\TEH ()11:\U l ,·
S,\~11'1.E l'RIORI I Y
BJIHl!/llNI: OU,11:RCil!N("Y
:•:~~~:~~t~RcS I c~c.1Rc11c:/c11c,c,c1cOcRcRc1c,----R•~iw,.,I 1
>flicc
BJ ("11,\IN or CPS l CllJY
E] SAr-11'Lll I YI'!: l)Aff. 7n~I
I l~IF.
rtJRN.ISI" o .. ,.,,
1 ,.._·~11on "' .Site
11,,.-,if'li<>n ,.,r <,,rnrli"ll point _______________________ _
S:1111plin1t ~le1hoJ
Rrm,,il,
LABORATORY ANALYSIS
DOD }10 not-I. lliu Solid, 70}00 mp,:L Ag-Sil-er 46S66
COD!li~H0 n1,i.·l. I luoriJe QS I m[l.1L ,\I-Aluminum 46557
COD Low JH m11-I. ll111dnrt! total'XJO mg!L As•Ancnic 4<,551
Cotifo,m MF fc-c:al }1616 /100.nl llaidntn (non-<:ub) 902 m1t•l. !Ja.lJaiium 46558
Coliform MF Tout }ISO.. 1100ml l'hcnol, J27JO ug.lL Ca-Calcium 46552
TOC m1t·l Sr«ific Cond 'H u,nhos/cm2 Cd·Cadiun1 -16559
lurt.itir-, NIU Sulfate ffi!!,'1, Cr-Chromium 46560
Rn.id""'. Su~ SJO "'Ill. Sulfide 7 4 S m!!.•L Cu-Copper 1042
TOW Su<pm<kd .,_Jidt mil 1-~IIIAS mg'L Fe-Iron l015
Oil 11nd G,e,ue m11JL II!.(• t-krcu,, 71</IXl
'" uni!\ Siliu "'f!-'L K·l'otnnium -1(,555
. .\llalinit.,. lo rll ~ S ,n,i:1. II""'" M11-• Mn~"nium '127
AlhJinill 10 pl I I J mitl. I onnaldeh, de mg:L ~ln•Man~C\J,ese 1055
Cat>c,na1c m!l L Nll,luN610 m,'L Na• Sodium <l2'l
11,cart>onat• 11111. L lt-NuNt.~S mwL Ni-Ni~~d
Cal;,on dio,iik m,i.1. S01 •N01 unfd0 mg.'L ' l'b-1.ead ~(,S(d
Chlooidc mp.I. ,, I otnl '" I' (,(,5 "'!t·L Sc-Selenium
0,r,:,mivm 11,. 101! u11. I. l'l)I mt1-I. /.n 7.inc -tr,Si,7
Colflf Jruc,~O '"
C1anidr7~0 l!lll [_
1,g.1L
ug/L
u&IL
u&1L
msfl.
ug/L
ug/L
u~L
"g/L
"WL
mf!)L
,,,,,.11.
ug.lL
111!!,'I.
ui,JL
<10 u,.:•L
u,:•L
u,.:•L
l ,,I, Nn,n!.,·,
ll.,1c H,·, ci,,·,I ;1111•111
1 imc RccciHd
Organochl111i11c l'cslicidcs
!JS
<"/1101'111
Org:rnophosphorus Pesticide~
Nitrogen l'es1icidcs
Acid llcrbicidcs
ScmholJtilcs
I l'll•Uicscl Ra11gc
\'olaiilc Organics I\'(),\ bo1tlc)
11'11·11 I EX tiawlinc K.m~c
I
Norlh Carol Ina
OUN-DVVATER FIELD/LAB FORM ~ . Deparlrncnl of F.nvlronmenl, He.11111, nml N;ilural nesources
DIVISION OF WAT En QUALi! Y · GllOUfHJWAT Ell SECIION ,·
SAMPLE TYPE
uad No L '-~ '.} 3 Serial No. ______ _ gw,,,;;-
Dsoll
0 Olher
SAMPLE PlllOlllTY
,gRout;,;;---
0 Emergency
(;·, Lab Number __ (.;_\ r7 Cz 1
) /4 -,.-;i)
@ Dale 11cr~~Jg_(Tu..-l nne ~;.,c-'_1 _ _ci.,o=--
al. 35'-•1 l-0(:, Long. 80 -~B · o-z... Rec'd by ' ___ r,0111 B11s~ei'. Ha11cl LJ
-----------• . Oilier: ____ _
Sch a In of Custody Report To: Ano. FR~1no. wano. Wino,
WSRO, Kinston FO, Fed. 1 rust, Cenilal 011 .. Other: _________ _
.'.>, Data Entry By _______ Ck: _____ _
_,. I ~Dale Reported _____________ _
Shipped by: Bus, Courie land Del., Other_· ____________ _
Colleclor(s): ~ f'1c(Li:, Dale l /1 ('18 PurposJ?:
·1 i111e _O_'!_II ____ Baselin~:;omplirrncn,_LUST, Pesticide Study, F,~dPi;11 I rosl, 01/mr: _____ _ -r ~ (cucl,..on<') FIELD ANAL Ys..E_!;i
pH,00 ---~_Spec. Cond 01 55 at 25° C
Temp.10 I 0 c Odor -~1-l~::>~!J_~ ___ _
Owner -.JO rlk.l ~(;°W;LOL!.'H~_,,w,..,,_.1"'"-"'""~-------------------
Location or site 15 2. LA 1'1/l~;"--'2,.., r,1f;',, Sir.JS,'<.,~ IJ,'-'-<~---'-Z.=f_.$c.'P=·~~~-
Descriplion of snrnpling poi11l 11'.o ".i ~(, /\T t, ..... , .. r..... ~·-/ T.~" · tc-Y--
Appearance-~-------------
Field Analysis By·
S.irnplinn Method pu MP ("""~,.i,a,i,,, ... ir.) Sarnple l11tc1vc1l __ i/~"~'~;AJ~. __
f1P.111r1rks < -
LABQRATORY ANALYSES £' r r o1 t::iW ,:, h le,-'<~ ll 1 \o-, (pun•p"~I I"""·.,,, Tntt'!' l'h:)
BOU, 310 my/I Diss. Solids 70300 rng/1 Aq -Silve1 11G5GG uq(I_ ~!_ff·1r1od1lori1H.? l'n;;lici1les ----
GOU I lic1l1 1so mnll Floulidc 951 mg{!_ Al -Alu111i11um -16551 uyll Orgnr1011l10spl1rJ111s l'1islicides -------· ----
GOU Low Jl5 ~~y~I_ 1J~1-!...dJ.l.c_s_s: 1 ulal 900 mg/I As -Arsenic ,1G551 uy/1 Ni!royen Peslicides ----
Coliform: Mr fecal J1G16 /1001111 I tc1rdncss_(11011-c.11lJ) 902 rnq~ Ba -lJnriu111 •1655fl uyll Acid I tcrlJicidcs
·-----·· ----·
Colilorrn: Mr f olnl :11~0.1 /l()(Jrnl f}!JC!1U!_S_J2_!.J(,) U~!I_!_ ~I-~ -C;1lci11111 •1G5~i2 lllfl/1 l'CIJ's --·--------·-
TOG GOO 1~19_11 Sµc_cjl_i.c_C_Q,ltL!J'..i l!ML1_QS[(.;IJ -'~ -~lL::..!~.~•!lrniwn -1GJ'.iU l!!l/1 ------···
~~idily 7G NIU §..t!)~nlc a,15 11.)/11! Cr -Ch10111iur11 ,tG:,r;o u1Jll ------------·--·------------
flc$iduc .. Suspendr•d !ilO lll[JII Sullklc 7,15 rnq/1 Cu -CU/!J!Cr -1GJG7 11y~I --------· -------·
' Fe -Iron ,\G~,GJ uy~ ~)r!111iv11l;ililr~ Urqar1ir:s -----··---· ---------------
011 and Grease mg/I Ilg -Mercury 71!JUU uy/I -, PH ~ Dies cl nanye --
pll <OJ unit: K -Potnssium t1G555 1119/1 <
--
Alkalinity lo pH '1.5 S 10 lll~l~ Mg -r..-1aqnesiurn -1655-1 mq/1 --
Alkalinily to pH 0.3 415 mgtl Mn -Manganese -16565 uy~ --
Carbonnle ,1,15 rngtl NII, as N 610 mg/I Na -Sodium •16556 lllfl/1 Volatile Organics (VOA IJo\lle) --
Bicarbonale -1-10 ITl(]/1 J KN as N 6"" ~1Q/l ..!li..c.l'fu;)s_el U_o/J TPH • Gasollne nange g --
Carbon dioxide -105 mg/1 NO, + NO, as N GJO mg/I Pb -Lead ,1656•1 uq/l TPII -UrEX Gasollm nange --
Chloride ~MO my/I P: lo/al as P 6GS mg/I Se -Selenium ug/1 --
Chromium: Hex: 103? uy/1 Zn -Zinc -16567 uq/1 --
Colo,: True BO cu --
Cyanide 120 111g/l
GW-5'1 11EV for Dissolved /\nnlysis -submit lilti:?1~d s;imple ~ml write "DIS" in .. a.k.
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GROUNDWATEn r::IELD/L/\IJ FOnM '
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IJIVl~.l<Hl <Jr'. V.'/\IFII llll/\.1 tl'i !:IHJI/IIIJ\N1\IFII ~;1:1:1H111
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111:.111
1.1•.1il
\ I ~ /' I
11'.fl
1111 I
>, ,1111' !" i ,'II Ill• 1·1 .__.._ ____________ ___, ,__.._ ____________ _, '---'----------··------·-
i
( 11, ,, II II n Id, If II p' ! ', • .Iii 1, I,",
( 11 ! 1;11 II'! ,I!' I' ·I ,t I' ,111•; f 1(' ;Ii, .i1 !,
I Jil11 !1 f1"1 I I,, .. ;111.i, I,:·;
/\1 :if l I lo •1 I 11, 11 I• .. ;
1.'1ll;1ltl•~ f J1q;111ic:; (\I( l/\ !u11\l,:)
lf'll-lla:;olln1! IL1tl(J(!
1 I '1 I · I I I I'. X ! ;:1•;nll1 •~ I 1;1n111:
tll'}.'JY
U.4U t-.'O
•
IJU.IH.1.1.
1)1\'ISltl,"\' OF \L\ I 1:H <Jll,\1,1 I\
f1,i \ \ \ : 3 2 ( 'h,111i,1n l.•I"" "l"', llqu>t r I 1;,,,..,,.J \\"n!rt ()11nli1.,
SAMJ'I.F l'KlORI I',
~Kc1u11N1: Ou.11:1rnu-.;c·y
r:roRT TO -·'-'-"-'-'---~----K,~,,,,,~1 Ollin
Ul.l.F.CTORl~I ),,;Rt:IIS.'~IOHHIS
EJ C"ll,\INOFCU!--JO[)Y
@J S,\/-11'1.E I Yl'E .\l E 7(:1"11
l\lF.
URPOSE JOHN 1.,\,\11\Ell I II \\'1:1,1.
1 ,,;;.,ti,,n .,, Si1r
lks.;riptu•n ,,J '-"l.mplinp ,,.,int _______________________ _
Sarllpliu~ Mr1l",J
ltrrn~,1•
,,\IJOIL\TOH\' ,\N,\LYSIS
DOD JIO '"• L !Jin SnliJ1 10Joo m;z;,L
CUD ll,11,h J~O mit·L I luoriJc Q51 m;z;:L -\1.-\luruinum 46557
CODU>"' JH mp.I. 11:uJncu h•lal ')O(l n•;t•I. l\s·,\rsrnic 46551
Coliform MF h-cal Jl(,lt, ll!~>inl lb,ilnen (non-carb)Q()2 rn1,1/I. 11:i•llarium 46558
Colifotm MF Tt>tal 1150-I 1100ml 1'11cnol1 J 2 7 JO u;:•L
IIX '"Ill Sr'("cilic Contl <JS umho~·n,.2
Turt-i1,1, t-:IU Su!f.llc m;:·L
RMid~ .Su'{'Cntlc-dSlO "'P-'L Sulli,k HS m;:'L
lt;>C.alSu~ .. ,1,d1 "'Ill. ~111,\S rnwl. J'c-loon l(JtS
11,I ruul (i1c.-uc 111!!.'I. 11!1,-Mc,c,111· 71900
'" '""" S,l,c:. mwl.
.\lhlinih In rll ~ ) n,11.\ """"'
.A.lhlinih IO rll ! l "'I'-I. I o,m;iltldntle Ill!('].
l•oonalc m11.l. :--1111nNMn m;t·I.
lliu,bo<wc mill. Ii,..::--,.• n1 N h:'.5 11111.'L Ni-Nkld
(·•ix., d,o,.Je m11-I. '.;o: •t,;01 a, n hW n,;z;•L
Chl(Ni<k '"fl-I. r 1,,1al ;i, I' <.,,5 m1,1L Sr-Selenium
Chn,mium lk, 10.11 Ufl-J. l'IU mwl. l.n Zinc -1/,St,7
C(>lor True ~u '"
C~anlJe 1:0 11'1t1.
m;tL
41 uwL
ug'L
SijMD;,
~----1.:oh :,1,.,,,1,.., HC; I ::;1,.J
1!.,lr lln,·,,,-d ;,R.''fR
1):,1" rq>ntkd
<l11,1:inochluoinc l'csticitles
PS
!lS
'1/101')~
Orgar,o;,hosphorus l'cslicidcs
Ni11ogeu l'cslicitlc~
,\ciil llnbiciilcs
\'ol;uilc t h1<~1,in (\'(J.\ 1,.,11k)
I 1'11-ti:i·.,,lii,r l(,.,wr
I l"I 1-1111:.'< ti,,-,.,liuc l{,,nf'C
Se-p tic.. ·i:; "k.
• Se.r-V IC. e__
;ROUNDWATER FIELD/LAB FORM\_,l·IAI N OF CUSTODY
SAMPLE TYPE SAMPLE e_rnornu ~ 'vV---;,-~ Enoutlne
D Soll D Erneruency D Ollrer _________ _
flep01I To: /\110, rii~rno, W,illO, WillO, ~-Chain of Custody
WSflO, Kinston ro, Feel. I rusl, Cenlral 011., Ollrcr: __________ _
Shipped by: Bus, Courie l,irul IJel, OIiier_· _____________ _
Norlh C.1roll11n
Uepml111enl of Envlronrnen1, He;ilt11, nml tfolural 11esource9
DIVISION or W /\TEil QU/IU rv -nnoutmw 111 Ell SECIIOt1
0 llata Entry lly: ________ Cle ______ _
l )ale Hnpor led: __________________ _
Prnposn:
Colleclor(s): k.JZt:t.6 /ltolt.U Dale J_Llf-<t-1;,'-------1 irnc _ __,_O'---'l-'----'o'--1.."-, __ lla:,elir1~;rn,111li.ir1cn, LU~r. P1i!;licirle St111ly, r1:cl1!1;1I 1111:;I, < Hl1ri1: ~ ~ lttr(lfl()lll') FIELD ANALYSES Owner o_r-J,._\ _ lA,:,_".£l01TII _w,,-,~ ______________________________ _
l.ocalion or ,;itc ___ J5.L'="1".Yh::r{Jl(_,('.c,l,1c:_/J.,_;,,£c1 Sllf!Clc'{,c:__ IJ,,_ _ -Z,_f]'p] J
Description of s:irnpli11u poinl _l-lrur;-l~_dz .. L .. 1!.T_b~<-f.: ,;/ r.--.... i<.l!"--yt_
pH.too _____ Spec. Cond.!J.\ /L{D al 2:,° C
Sarnpli110 Mrilhod ____ l)L},IV\~ -···--··-··---·-· ------~-:;;11111111? 111\!!rv:il _____ Q_!'-.c''-'·,..,=----f-!1'1111,p_ Jo;ul,•1. olc J
rernp Zr 0 c Odor -~f.J~•~)~!J_s.--___ _ ·,o
Appern rn,co _gr.N ___ _
rler11a1ks -----------------~-~~~-----------------(1,,,,,,11,,~11orn1', ~•• lomp f'lr:) Field Analysis lly: ---~(_),~~--------
LABORATORY ANALYSES -f ~-1 FTu.J t:: ' l'l, .J-' l:L\J.Q
UOlJ. 3,0 ll)!J!! U!ss. Solids /UJOO mq/1 ~fl -Silver ,1G5GG uu~ Q~uar10d1lori11e l1eslici1les ------
COlJ I ligli J,10 rll!J/1 Floulic..le 951 111f.11_ ----/\I -/\lu111imn11 ,w55/ uv{! 01!.JiHHJl,l u l:;1111or 11s I 'r!slicilles -----
COlJ Low 335 lllij/\ !J~!.!l!leSS: -, u\nl 900 1u.uLL As -A,senic •1G551 uq/I l·lilrouer1 l1cslicidcs ------
Colilmm: f.1F Ft•c:al 3IGl6 /1001111 ll;irdness {!1011-cc11ll) 902 -----11 l(j{!_ Ua -8c1riu111 4G558 uy,:i_ Acid I led,icidcs --
Colilur111: r.-1r-lol;il 31!1lJ.1 /1 UOrnl Pt1c11ols 32730 -· uu[L Ca -Calcill(!l ,1G552 ll~f!(I PC(l's ------TOG GOO r~HJ'.! --sm~i;i!lG.C:Yl!_tJ_vs tJl:-.Um~lQ•f --Cd -C_c:uhnit1111 '1G55a uql! ----
___!_~1~:i0~t /G 1-J I lJ ~!!!!~\le !J.15 rnq/!_ Cr -Cl110111i11111 ·1G5GU ULJ(( -------------· ··----------------
llcsldue., Su~p1md1id ~.:Jo lll!JII !)11llide /,15 rnu!J. --Cl_! -Co1!pcr •IG!.iG2 ll!.J!J ----re~ hon '1G5G3 ll\l{! Sc111ivola1i!{! 01!_J<1r1ir:s ---------
OH and Grease ll)U(!. _llu_-Mmcury_7ViJOO ~~JI' TPI I -Illes el Flaoue
------------------·~-----·-·· --------------· ----·------·-· ··---------
pl I ,tUJ unili I< -11o1<1ssiurn '11i~55 111!.JII --------/\lk;ilinily lo pl I ,1_5 ,t 10 111\JI~ --____t:!g ~ Mau1icsiurn ,155~,1 11 )!J~l ----/\lk;ilinily lo 1!1 I !l.3 ,I 15 llli!~t _ Mn -M.111ua11ese ,1GSG5 ll!.Jll ----
CnrlJmrnlP. •l-15 rnotl UJ\_{!S M G ID '!!!JI!_ t·Ja -Sodi11111 •1GSSG 111!.J(I Volalil!J O~q:111ics (VOA hollln) --------·------8icarl.Jor1ale ,1,10 mutJ --J l\tl.as.N . ..fi"" 'llU/1. g JJU:!i<;ll.c' u\11! --TPII -Ga~oll11e_fla11ue -
Carllon dioxide ,10:, lll!JI~ !:!Q"'__±_UQ~..i!~ r.J 630 111q(L PlJ -Lead ,\G56·1 U!J~ --TPI I -f) I EX Gasolhr._nanije --
Chloride 9.10 lllY!! P: ·1 otal as P GG5 rnq/I Se -Selc11i11111 uqtl --
Cl110111iu111: I lex 1032 uul_!. Zn -Zinc •1G5G/ uq/I --
Calm: True BO cu ----
Cyanide /20 I null
Lab Cornrnenls:
GW-5'1 f1EV. 71% Fu, Dissolved J\11;"tlysis -s11IJ111it lillcrcd snmplc c1nd wlilo ''DIS" in t,i,..,:k.
COUNTY
QUAD NO
-"-"_:,,_E,_ ... ___ ~q~s rEB 20 Pl\ iz: 20
REPOR"J TO _,_1_1<00 ________ Regional Office
~~~-:;ECTOR(S) · ,'c",c~"l, .. 01~0~90~~------
T!ME:
PURl'OSE: Owner:
Location or Site:
Ul\'ISION OF WATER QUALITY
Chemistry L1bonlory Rrporl / Ground ,vnter Quality
SAMPLE PRIORITY
~ltOUrlNE □EMERGENCY
~ CllAINOFCUS-IODY
0 SAMPLE TYPE
JOIIN LAMBETH
□
Description of sampling point _______________________ _
Sampling Method·
Remarks·
LABOIUTORY ANALYSIS
lJOVJIO mg/L Ois~i. Solids 70300 mg/L Ag-Sih·er 46566
COD lligh 340 mg/L Fluoride 95 l mg/L Al-Aluminum 46557
COD LowJJ5 mg/L I lardness: to1al 900 mg/1. As-Arsenic 46551
Coliform: Mt'l'.-.:al31616 /IOOml Hardness: (non·c,,,b) 902 mg/L lh-Bnrium 46558
Coliform: MfTotal 31504 1100ml l'hcnols 32730 ug/L Ca-Calcium 46552
TOC mg/1 Specific Cond 95 uruhos/cm2 C<l-Cmlium 46559
Turbitity N"IU Sulfate mg/L C,-Chromium -16560
Residue., Suspended 530 mg/L Sulfide 745 mg/1. Cu-Copper I 0-12
fotal Suspended solids mefL MIJAS mefL Fe-lronl045
Oil ru1d Grease mg/L Ilg-Mercury 71900
pll units Silica mg/L K-Potassium 46555
Alkalinity lo pll 4.5 mefL llornn Mg· M:igncsium 927
Alkalinity 10 p!I 8.3 mg/L Fmmaldehyde me/L Mn-Manga11cse 1055
Crubonate mg/L NHJ as N 610 mg/L Na-Sodium 929
Uica,bonalc mg/L TKN as N 625 m;:/L Ni-Nidd
Crubon dioxide mg/L N02 +NOJ as n 6JO msJL X Pb-Lead 4656,1
Chloride mg/L r: Total as I' 665 mg/L Se-Selenium
Chromium· /lex 1032 ,efL 1'04 mg/L Zn_Zinc 46567
Color: True 80 " Cyanide 720 mg/L
CO/\II\IENTS:
26
~rc=======a
ug/L
ug/L
ug/L
,g/L
m;:/L
ug/L
uglL
"g/L
,g/1.
ug/L X
mg/L
m;:/L
,giL
rng/L
,giL
ug/L
ug/L
ug/L
Lab Number 7G2667
Dale Received : 12116/97
Time ReceiHd : 9; 15
Re.:eh·ed By OS
Released By OS
Date reported: 2118198
Organochlorine Pesticides
O,ganopho~phu,us Pesticides
Nit,ogcn Pesticides
Acid I lc1bicidcs
Semivolatiles
!"Pl I-Diesel Range
Volatile Organic.~ (VOA bottle)
J'l'II-Gasoli11e Range
Tl'II-UTEX Gasoline Range
7G]667.0EC
Norlh Carolina GROUNDWATER FIELD/LAB FORM Department of Environment, Health, and Natural Resources DIVISION OF WATER QUALITY· GROUNDWATER SECTION
County 5,-" cl,, ii
Quad No L 6 7•j ; Serial No.-,,--,-,-----,,---
Lal. 3 .t'"' '.:( J' ob "IV Long. 0o" ')8' c). "U
Report To: ARO, FRO(§h, RAO, WaRO, WiRO,
SAMPLE TYPE
i2!Water
□soil D Other
SAMPLE PRIORITY
f:I'Routine
D Emergency
----------
. Chain of Custody
WSRO, Kinston FO, Fed. Trust, Central 011., Olher: _________ _ 0 Other: -----------'--------
Dala Entry By: ______ Ck: ______ _
Date Reported: _______________ _
Shipped by: Buj).C~ Hand Del., Other·_-. __ -, _________ _
I , [ ( ,_ •1 / i./ :;c, Purpose:
Colleclor(s): "' e...__ Date O (If L1 I Time --'----''=~[~f:=i~B~a:s•:l;in;e~, Cform:pl=a~in~l,~C=o~m~p:li=a~nc~e~,=L:U~S=T~, ~P:•:sl:ic:id=a~S:l:u~dy~,~F~e:d:e~ra~I ~T~ru=s~t,~O:l~he:r~: ~~;;;;~~t= FIELD ANALYSES · / 1 fJ Owner_ c-~ &._,.,, 6"-rt '""'"'"'' '' pH400 s--s: :(~ Spec. Cond.94 :SI aL.zso C Location or site __ L_,-:.-.g>~1_,., __ ;:d~---.--,-~---,-~-,---,----------------Temp.10 / S 0 c, Odo!., Description of sampling point -~-"c,;r:c..c,'i,f'k"--'i_,,,s:c..f'-_b.c.c"c~k.---=~4,J-:cc"--'--f-'-r_•_c1c..l,_,...=---------------Appearance c Uu:.---_L:;·'•l-(.,, Sampling Method ---=-.--,,a':;;;-hc==.--------Sample Interval ________ _ Field Analysis By: ---=Y~•c~b~l~e.._~~-------Remarks lc-6 ..-<-. ~ >i.... _-~••'~·"'·' LABORATORY ANALYSES (pumpi"''"''·''"""·"''
BOD. 310 ma/I Diss. Solids 70300 moil Aa -Silver 46566 ua/1 Organochlorine Pesticides COD High 340 mg/I Flouride 951 mo/I Al -Aluminum 46557 uq/1 Organophosphorus Peslicides COD low 335 mg/I Hardness: Total 900 mo/I As -Arsenic 46551 ua/1 NilroQen Pesticides Colilorm: MF Fecal 31616 1100ml Hardness (non-carbl 902 ma/I Ba -Barium 46558 ua/1 Acid Herbicides Colilorrn: MF Total 31504 1100ml Phenols 32730 ua/1 Ca -Calcium 46552 ma/I PCB's TOG 680 ma/I SQ!~Qific QQnQ, fJS uMho~:b;;;m2 Cd -Cadmium 46559 ug/1 Turbidity 76 NTU Sulfate 945 rnn/1 Cr -Chromium 46560 uo/1 Residue., Suspended 530 mg/I Sulfide 745 ma/I Cu -Conner 46562 ua/1
Fe -Iron 46563 uo/1 Semivolatile Organics
011 and Grease mq/1 Hg -Mercury 71900 ug/1 TPH -Diesel Range pH 403 units K -Potassium 46555 mg/I Alkalinity to pH 4.5 410 mg/I Mq -Maanesiurn 46554 ma/I Alkalinity to pH 8.3 415 mg/I Mn -Manqanese 46565 uo/1 Carbonate 445 mg/I NH as N 610 mo/I Na -Sodium 46556 mo/I X Volalile Organics (VOA bollle) Bicarbonate 440 mail TKN "0 N ,::')r:;: moll bli -~i~~el uotl TPH ~ Gasoline Ranae Carbon dioxide 405 mg/I NO. + NO as N 630 mo/I -x Pb -lead 46564 ua/1 TPH -BTEX Gasollre Range Chloride 940 mg/I P: T olal as P 665 malt Se -Selenium ua/1 Chromium: Hex 1032 ug/1 Zn -Zinc 46567 uo/1 Color: True BO cu
Cyanide 720 mg/I
Lab Comments: -----------------------------------------------------------
GW-54 REV. 7/96 For Dissolvod Analysis -submit fillered sample and wrile "DJS" in block.
EHNR/OWQ LABORATORY LAB NO. 7G2667
VOLATILE ANALYTICAL REPORT
RL'l'>ORTED BY ~ SUPERVISOR
CHECKED BY
REVIEWED BY
ENTERED BY
SAMPLE TYPE: WATER ANALYSIS RESULTS
75-35-4 1, 1-0ichloroethene 0.75 u 96-18-4 1,2,3-Trichloropropane 0.25 u
75-09-2 Methylene Chloride 10 u 108-86-1 Bromobenzene u
156-60-5 lrans-1,2-Dichloroethene 0.75 u 95-49-8 2-Chlorololuene 0.25 u
75-34-3 1, 1-Dichloroethane 0.25 u 106-43-4 4-Chlorotoluene 0.25 u
590-20-7 2,2-0ichloropropane 0.25 u 541-73-1 1,3-0ichlorobenzene 0.25 u
156-59-4 cis-1,2-Dichloroethene 0.25 u 106-46-7 1,4-Dichlorobenzene 0.25 u
67-66-3 Chloroform 0.25 u 95-50-1 1,2-Dichlorobenzene 0.25 u
74-97-5 Bromochloromethane 0.75 u 96-12-8 1,2-Dibromo-3-Chloropropane 1 .u
71-55..S 1, 1, 1-Trichloroethane 0.25 u 120-82-1 1,2,4-T richlorobenzene 0.25 u
563-58-6 1, 1-Dichloropropene 0.25 u 87-68-3 Hexachlorobutadiene 0.25 u
56-23-5 Carbon Tetrachloride 0.75 u 87-61-6 1,2,3-T rich!orobenzene 0.75 u
107-06-2 1,2-Dichloroethane 0.25 u 1634-04-4 Melhyl-tert-butyl ether 5 u
79-01-6 Trichloroethene 0.25 u 71-43-2 Benzene u
76-87-5 1,2-Dichloropropane 0.25 u 106-68-3 Toluene u
75-27-4 Bromodichloromethane 0.25 u 100-41-4 Ethyl benzene u
74-95-3 Dibromomethane u 108-38-3 m.p-Xylenes 2 u
10061-01-5 cis-1,3-Dichloropropene 0.25 u 95-47-6 a-Xylene u
10061-02-6 trans• 1, 3-Dichloropropene 0.25 u 100-42-5 Styrene u
79-00-5 1, 1,2-Trichloroethane 0.25 u 96-82-8 lsopropylbenzene u
127-18-4 Tetrachloroethene 0.25 u 103-65-1 n-Propylbenzene u
142-26-9 1,3-0ichloropropane 0.25 u 106-67-6 1,3,5-T rimethylbenzene u
124-46-1 Dibromochloromethane 0.75 u 96-06-6 lert-Butylbenzene u
106-93-4 1,2-Dibromoethane 1 u 95-63-6 1,2,4-Trimethylbenzene u
106-90-7 Chlorobenzene 0.25 u 135-98-6 sec-Butylbenzene u
630-20-6 1, 1, 1,2-Tetrachloroethane 0.25 u 99-87-6 p-isopropyltoluene u
75-25-2 Bromoform 0.5 u 104-51-8 n-Butylbenzene u
79-34-5 1, 1,2,2-Tetrachloroelhane 0.75 u 91-20-3 Naphthalene u
mg/l mg/l
TQL-Target Quantitation limit-Subject to 0.25 N
change due to instrument sensitivity
T-Tentatively Identified, not confirmed Detected
E-Estimated Value ug/L
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound NO VOLATILE ORGANIC COMPOUNDS
0-Detected below quantilation limit DETECTED BY GC/ELCD/PIO.
M-GC/MS Analysis performed
COMMENTS:
COUNTY
QUAD NO:
_ll_<E_OJ_CL_L _~9~8~f-_· EC 2 0
UIVISION OF WATER QUALITY
Cht'111islry L111Jor11tory l{rport / Ground WR!rr Quality
SAMrLE rRIORITY
[R)ROUTINE □EMERGENCY
REPORT 1 0 0,0101<0o ________ Rrgiona! Office [RJ CIIAIN OF CUSTODY
E] SAMrLE TYPE □ COLLECTOR(S) s"c'c"='""=··=·N'------
D,\ 1 E: 12/15/97
TIME:
l'URPOSE· Owner: MELE POTTS R~;s
Lm:ation or Sile:
Description of sampling poinc _______________________ _
Sampling Method·
Remaih·
LABORATORY ANALYSIS
80[) 310 m"'1-Diss. Solids 70300 m"'1-Ag-Silver 465(,6
COD High 340 mg/I. Fluoride 951 m"'1-Al-Aluminum 46557
COD Low 335 m"'1-I lardness: total 900 m"'1-As-Arsenic 46551
Co!ifo,m: MF Fecal 31616 1100ml Hardness: (non-carb) 902 mg/L Ba·Barium 46558
Coliform: MF Total 31504 /IOOml l'hcnols 32730 ,.,,,_ Ca-Calcium 46552
TOC mg/I Specific Cond " umhos/cm2 Cd-Cadium 46559
Turhi1i1y NTU Sulfate 11,g/L Cr-Chromium 46560
Residue., Suspended 530 m"'1-Sulfide 745 mg/L Cu-Copper 1042
Total Suspended solids m"'1-l'-WAS m"'1-Fe-11011 1045
Oil and Giease m"'1-Jig-Mercury 71900
pll units Silica mg.IL K-Potassium 46555
Alkalinity to pll 4.5 mg/L Boron Mg-Magnesium 927
Alkalinity to pH 8.3 m"'1-Forinaldehyde m"'1-Mn-Mangane5e 1055
Cnrbonme m"'1-NIIJ as N 610 mg.IL Na-Sodium 929
Bicarbonate mg/L TKN as N 625 m"'1-Ni-Nickel
Carbon dio:<ide m"'1-N02 +NOJ as n 630 m"'1-X l'b-Lead 46564
Chlmide m"'1-r. Tolal as I' 665 mg/I. Se-Scleniu111
Chromium Hex 1032 uglL P04 m"'1-Zn Zinc 46567
Color: T,uc 80 rn
Cyanide 720 mg/L
COMMENTS:
Ulb Number 7G2666
Date Received 12/16/97
Time Received 9;15
Received By vs
Released By DS
Dale reported : 2/18/98
,g/1. 01ga11ochlorinc resticides
,g/L Orgarmphosphorus Pesticides
,g/L Nitrngcn res1icidcs
,g/L
m"'1-Acid llcrbicides ,.,,,_
,g/L Semivolatiles
,g/L Tri I-Diesel Range
,g/L
,g/L X Volatile Organics {VOA bottle)
mg/L
m"'1-rrll-Gasoline Range
,g/1. TPl!-BTEX Gasoline Range
mg/L
ug/L
23 ,g/1.
ug/1.
ug/L
7G1666 DEC
, . .
•,, ,1 -'/ .·1 ·1 '\ ,. Nor I h Carolina -~· ··., I'
GROUNDWATER FIELD/LAB FORM ·--~f_;',1<\/;i,} I;" I -(.~
1f_f:\·':;· '.' ,,-. ~ ~ Department of Envlronmenl, Health, and Natural Resources ·l : :. ) )' , I DIVISION OF WATER QUALITY· GROUNDWATER SECTION
Counly ;:;.,..Llt SAMPLE IYPE SAMPLE eBIQRIIY Lab Number • (( 1
-< cJ, r n( n I()
Quad No Ll 7~ ,), 'i'. Serial No. ·E':f Water Ef'Routine Dale Received I Jj 1 (g r:1T;m~_0.-I '7 ~ f'' 7'.3 :,.( 5 ,, N ,:, c/' re I C{ '' lJ 0 Soil D Emergency 0 Rec'd by: ')[Ys' From: Bus,6uri~ Hand Del., Lal. .> Long (,, , D Other
Olher: ,,.---, )E1 Chain of Custody Ck: Reporl To: ARO, FR~, RAO, WaRO, WiRO, Dala Entry By:
-WSRO, Kinslon FO, Fed. Trusl, Central 011., Olher. _________ _
Shipped by: Bus,_~ Hand Del., Olher_· -~----------). ; · / / ·1-, '/ • -Purpose: / .· JLL)2.._ Colleclor(s): I "h l'S-, Dale 21> '1 7 Time /· 2 i Baseline, Cfmplainl, Com7ia;ce, LUST, Pesticide Sludy, Federal Trusl, Olher: -=u-'-'-W--\----'--7'----'--/ j ( . . _ (cncloono) -t / I_ · FIELD ANALYSES Owner ·, e c."\· / -;&.,,, "-. 1e...,<. c,·,~.,.., i~ -,;.,Nu>/
pH400 5--r:-5-Spec. Cond.94 'I~' al t/o C Location or sile /-'-S-u 6-Ji:/s· &d / 5 C.: ·e[u Ci.,_
Temp.10 /'-f 0c. Odor Descriplionofsamplingpoinl __ .,_/.,=·.,,·'-':a·ut:c, _______________________ _
Appearance c.· /.,_,.;-~,i (.:: -{_,_,-.r Sampling Melhod ----~--~=-==~-------Sample lnlerval ________ _
/ ( ( ( ,--/(Pumi:»Oador, olc.) Field Analysis By: ch "'-Remarks v:· "~-~) "' c:.....---
Date Reported.-------------;:_::_-::_-~,,
LABORATORY ANALYSES trium11mo limo, air lomp. olc.)
BOD. 310 mq/1 Diss. Solids 70300 mg/l An -Silver 46566 ua/1 Organochlorine Peslicides
COD High 340 mg/I Flouride 951 rno/1 Al -Aluminum 46557 ua/1 Organophosphorus Pesticides
COD Low 335 mg/I Hardness: Total 900 mg/I As -Arsenic 46551 ug/1 Nitroqen Peslicides
Colilorm: MF Fecal 31616 1100ml Hardness (non-carb) 902 mn/1 Ba -Barium 46558 ua/1 Acid Herbicides
Coliform: MF Total 31504 It 00ml Phenols 32730 ug/1 Ca -Calcium 46552 mq/1 PCB's
TOC 680 rnq/1 Sge~ific CQnd. 95 uMho~l~m1 Cd -Cadmium 46559 ua/1
Turbidity 76 NTU SuHate 945 mg/I Cr -Chromium 46560 ua/1
Residue., Suspended 530 mg/I Sulfide 745 mn/1 Cu -Conner 46562 uq/1
Fe -Iron 46563 ug/1 Semivolalile Organics
Oil and Grease mall Hg -Mercury 71900 ug/1 TPH -Diesel Range
pH 403 uni!~ K -Polassium 46555 mg/I
Alkalinily lo pH 4.5 410 mg/I Ma -Maanesium 46554 mq/1
Alkalinily to pH 8.3 415 mg/I Mn -Manganese 46565 ug/1
Carbonate 445 mg/I NH as N 610 mn/1 Na -Sodium 46556 mq/1 ---,.,c· Volatile Organics (VOA bottle)
Bicarbonate 440 ·mq/1 TKN "'"' N &.'Jr:::.: "'o/L l\li. ,_,:~1-~t "n/1 TPH • Gasoline Range
Carbon dioxide 405 mg/I NO + NO as N 630 mall X. Pb -Lead 46564 ug/1 TPH • BTEX Gasollre Range
Chloride 940 mg/I P: Tolal as P 665 rnn/1 Se -Selenium uq/1
Chromium: Hex 1032 ug/1 Zn -Zinc 46567 ua/1
Color: True ao cu
Cyanide 720 mg/I
Lab Comments:-----------------------------------------------------------
GW-54 REV. 7196 For Dissolved Analysis -submit filtered sample and write "DIS" in block.
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
75.35-4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-66-3
• 74-97-5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79-34-5
TOL-
T-
E-
U-
N-
D-
M-
COMMENTS:
WATER
1, 1-Dichloroelhene 0.75
Methylene Chloride 10
trans-1,2-Dichloroethene 0.75
1, 1-Dichloroethane 0.25
2,2-Dichloropropane 0.25
cis-1,2-Dichloroethene 0.25
Chlorofonn 0.25
Bromochloromethane 0.75
1, 1, 1-Trichloroethane 0,25
1, 1-Dichloropropene 0,25
Carbon Tetrachloride 0.75
1,2-Dichloroethane 0.25
Trichloroethene 0.25
1,2-Dichloropropane 0.25
Bromodichloromethane 0.25
Dibromomethane
cis-1,3-Dichloropropene 0.25
trans-1,3-Dichloropropene 0.25
1, 1,2-Trichloroethane 0.25
Tetrachloroethene 0.25
1,3-Dichloropropane 0.25
Dibromochloromethane 0.75
1,2-Dibromoethane
Chlorobenzene 0.25
1, 1, 1,2-T etrachloroethane 0.25
Bromoform 0.5
1, 1,2,2-T elrachtoroethane 0.75
Target Quantitation Limit-Subject lo
change due to instrument sensitivity
Tentatively Identified, not confirmed
Estimated Value
Samples analyzed for this compound but not detected
Sample not analyzed for this compound
Detected below quantitation limit
GC/MS Analysis performed
EHNR/DWQ LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RES UL TS
u 96-18-4
u 108-86-1
u 95-49-8
u 106-43-4
u 541-73-1
u 106-46-7
u 95-50-1
u 96-12-8
u 120-82-1
u 87-68-3
u 87-61-6
u 1634-04-4
u 71-43-2
u 108-88-3
u 100-41-4
u 108-38-3
u 95-47-6
u 100-42-5
u 98-82-8
u 103-65-1
u 108-67-8
u 98-06-6
u 95-63-6
u 135-98-6
u 99-87-6
u 104-51-8
u 91-20-3
1,2,3-Trichloropropane
Bromobenzene
2-Chlorotoluene
4-Chlorotoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene .
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
Hexachlorobutadiene
1,2,3-Trichlorobenzene
Melhyl-tert-butyl ether
Benzene
Toluene
Ethyl benzene
m,p-Xylenes
a-Xylene
Styrene
lsopropylbenzene
n-Propylbenzene
1, 3,5-T rimethylbenzene
tert-Butylbenzene
1,2,4-T rimethylbenzene
sec-Butylbenzene
p-isopropyltoluene
n-Butylbenzene
Naphthalene
NO VOLATILE ORGANIC COMPOUNDS
DETECTED BY GC/ELCD/PID
LAB NO. 7G2666
SUPERVISOR w(:.
DATE . · '7ff,
ENTERED BY
DATE
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.75
5
1
2
mg/L
0.25
mg/L
Detected
ug/l
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
N
North Carolina Department of Environment, Health, and Natural Resources
Division of Epidemiology
Occupational and Environmental Epidemiology Section Ji~ ~;),
Medical Evaluation and Risk Assessment Branch
Drinking Water Health Risk Evaluation
. General 'J;'~
County
DATE __ C/,__...ffc.,_f)~_ LABORATORYNUMBER __ '7-"-"'-!r_6~;~f~'-----/ __ _
() Based on these analytical results, this water should be considered safe for normal usage.
( ) Chemical analysis did not show any contamination. Water should be resampled if odor or taste
persists.
(X) The water should not be used for drinking or cooking purposes.
( ) Based on these analytical results, this water is highly contaminated and should not be used for
· drinking, cooking, or bathing/showering.
() The laboratory results are not conclusive, please resample.
PLEASE IND/CA TE ON LAB SHEET THAT IT IS A RESAMPLE AND PROVIDE PREVIOUS
SAMPLES NUMBER(S)
(X ) COMMENTS:
The nitrate drinking water standard is 10 ppm. The nitrate level in your well water is either above or close
to the drinking water standard. Continued consumption especially for pregnant women or infants six
months of age and younger may pose an increased health risk based on these nitrate levels
For further information, contact Or. Ken Rudo, Occupational and Environmental Epidemiology Section,
[phone]
DEHNR 3891 (1/96)
Occupational and Environmental Epidemiology Section (Review 1/97)
COUNTY
QUAD NO:
!REDELL
o·· ,1,v 1, -· I I Ii 1 , I f,'111=28
RErORTTO
COLLECfOR{S)
0,\ l E
_,,_IR_O _________ Regional Office
DA11LEN
4(7/97
l'l,\!E:
PURPOSE
LAllORATORY ANALYSIS
UUO JlO
COD fli!,lh J•lO
COO Low JJS
Cotifo,m: Ml' Fecal 31616
Coliform: /..1FTotaJJ1504
IOC
rurbi1i1y
Rc~iduc. Suspended SJO
rotal Suspended >ollds
pH
Allalinit)· to pH 4_5
A\~alinil) to pH lU
Carbona1e
llicaibonale
Carbon d10,1de
Chloride
Ch1rnniu,11 lk.xl0.12
Ct>lu, lru~ Ml ~
C1 an;,k 720
m)I/L
mg/L
ms.IL
1100ml
/IOOml
mgll
NlU
mg/L
mg/L
II/UIS
mg/L
mg/L
mVL
m.i;/L
mgll
mgll
ugil.
( u
rng.lL
Ov.ncr:
Location or Sile:
Description or sampling point
Sampling Method·
Remarks·
Uiss. Solids 70300
Fluoride 951
Ha,dness: total 900
lfard[lcss: (non-carb) 902
rhenols J27J0
Spe<:ific Cond. 95
Sulfaie
Sulfide i4S
MBAS
Oil and Grcn,e
Silica
Ilomn
Formaldehyde
NIU as N 610
lKNasN625
X N02 +NOJ as n 630
r: To1a! as r 665
1'04
DIVISION OF WATER QUALITY
Chemistry LabonlOf)" Reporl / Ground \\'11!cr Qunlily
SAMPLE P.ill.QB.JTY BJ ROUTINE
[] CHAIN OF CUSTODY
EJ SAMPLE TYPE
ALLEN CASCADDEN
mg.IL
mglL
mg.IL
mg/L
,g/L
uMhos/cm2
. mg.IL
mg/L
mg/L
ong/L
mg.IL
l]lg/L
0.01 mg/L
mg/L
12 m[;!L
<0.01 m[;!L
rngll.
□EMERGENCY
□
Ag-Sihcr 46566
Al-Aluminum 46557
As-Arsenic 46551
lla-llariurn 46558
Ca-Cakium 46552
Cd-Cadiurn 46559
Cr-Chromium 46560
Cu-Copper 1042
Fe-hon 10-!5
' t lg-Me,cury 719QO
K-Potassium 46555
Mg-'-1agncsiurn 927
Mn-Manganese 1055
Na-Sodium 929
Ni-Nic~el
l'b-Lcad 46564
Se-Sclcnlum
7-n Zinc ~65(,7 .
Lab Number 7GU781
Da1c Rccei,cd 418/97
Time Rccci,ed o.OOAM
Rccci,cd Uy us
Released II)· us
Date reported: S/1 J/9J
uglL Urganoch!orinc l'csticidcs
,g/L Organophosphoms Pesticides
uglL Ninogen l'csticidcs
ug1L
mg.IL Acid lkrbicillcs
ugiL
uglL Scmi,olatilcs
uglL Tl'll-Uicsel Range
ug1L
1.1 ugll. X \'ob1i!c O,gm,ics (\'tJ,\ bnltk)
mg1L
mg1L TPJI-Ga!,Olinc R;mgc
U!:!/L 1'1'11-131 EX Gasoline Range
m1,tlL
U):!1L
ug!L
U):!..'L
"!:!;l.
IGOf!I APR
Norlh. Cnroll11n
GFlOUMDWATER FIELD/LAB FORM . Dcpotlmc11l of E11vho11111e11l, llc;:11111, nruJ Nalu1ol '1csou1ccs
I • " ' .. :· ! ! 11 i ··01v1s10N OF ENVinor,MENfAL MAl,AGEMENT -GnourmWA1 En SEC110N :: '; .' ' . .' 'i
Serial No. _______ _ SAMPLE PRIORITY
-··----:--. ..
neporl To: AllO, FflO.~Rno. Wallo, Wino,
WSflO, l<inslon FO, Lli9· Trust, Cenlral OIL, OIiier:
Sliipped by: Bus,~, Hand Del., Ollier_· ___________ _ ;'\ ( 'I/~/ , J. Purpose:
Colleclor (s): .vch• <.60 Dale ~'t-r_L_ Time / · '-/6 Baseline, Complaint, Compliance _LUST, Pesticide Siudy, Federal Trusl, Oilier: LrL> '·""-"' J'fJ.2--
FI ELD ANALYSES Owner ~dJ.,.·-"'~~--....._-1
_"'_'"_'"_' ---,----,---------~---
pl·l,00 ~-s: J_.-Spec. Co11d.9, /(. O at~ C Location or site (,'. ..f I(
l:2JnoUTINE 0EMEl1GENCY
-~CHAIN OF CUSTODY 0
Lab Nurnbe~Q:1'6_\
Date lleceived h _ --\=ll--Time ci-c'·c!!.-'=c'.'....---
llec·d by:_ From: Bu DUii
Other: _________________ _
Data Entry By: ______ Ck: ______ _
. Hand Oel.,
Date lleported: _____________ _
Temp.10 c 0 c Odor_______ Description of sampling poinl _ __,c;,z;.~-'----'-'~--==='-'"'./="-.Ll'-""'-"-""---------------
/\ppeara11ce. ,C.<4--/~,J,-&✓-,,· Sampling Method_______ _ __________ Sample t11terval _______ _
Field /\11alysis By: '{)c;: t, Ce, 11emarks _.,_1"'-'--'"'-=~'--'--L,""-"------,===-==--=.------------------~-
LABORATORY ANALYSES (p,mpi"'"""·''"mp.,"·1
BOD, 3(0 mg/l Diss. Solids 70300 mq/1 Ag • Silver 4G566 ug/1 Organochloririe Pesticides
COD High 340 rng/1 Flouride 951 mg/I Al• /\lur11inum 46557 uqll Organophospho,us Pesticides -COD Low 335 rng/1 Hardness: Tolal 900 rng/1 As• Arsenic 46551 -ugll Nilrogen Pesticides
Coliform: MF Fecal 3161G 11 OOrnl Hardness (non-carb} 902 1119/I Ua • 8.:irium 4G550 ug/1
Colilor111: MF Tol.:il 31504 1100ml Phenols 32730 ugll Ca -Calcium 46552 mq(I /\cid Herbicides
TOC GOO rnq/1 5,gecilic Cond. --95 uMhos/crn] Cd · Cadmium 46559 ug/1
Turbidity 76 NTU Sulfale 945 mg/I Cr• Chromium 46560 --ugll Se111ivolatile O,ganics
llesidue., Suspended 530 rng/1 Sulfide 745 mq/1 Cu · Copper 465G2 ·ug/1 --
Fe -Iron 4G5G3 ug/1
~ Hg -Mercurt 71900 ug/1 x Volatile Organics (VOi\ boltlt?)
pH 403 units K . Potassium 46555 rng/1
Alkalinily lo pl-I ~-5 4(0 mg/I --Mg -Magnesium 46554 mg/! TPH • Gasoline Range
Alkalinily lo pH 8.3 415 mg/I Mn• Manganese 46565 ugll TPH -fff EX Gasoline nange --
Cmbonate 445 mg/! NI 1, --as N GIO 111911. Na -Sodium 4655G myll
Bicarbonate 440 ,ngi TKN as N 6?S •JlQ/1_ Ni. Nickel ug/1 -------
I Cai bon dioxide 405 mgil Ix _NO + N03 as N 630 nig/1 Pb -Lead 46564 ug/1 -----I / Chloride 9·10 rng/1 P: Tolal as P 6G5 mfl!'.l Se -Selenium ugll
Chromium: Hex 1032 ug/1 Zn -Zinc 465G7 uoll I/
Color: True eo Pt-Co
Cyanide 720 rng/1
Lab Comments:-------------------~------------------------------------------
GW-5•1 REV. G.'93 For Dissolved Analysis . submit !iltered sample find write "DJS'' in block.
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE
75-35-4
"/5-09-2
158-60-5
75-34-3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
553-58-6
56-23-5
107-06-2
79-01-6
78-67-5
75-27-~
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
i24-48-1
106~93-4
108-90-7
630-20-6
75-25-2
79-34-5
TOL-
T-
E·
LJ.
N-
0-
M-
COMl·.1ENTS·
WAlER
I. 1-0ichloroethene 0.75
Methylene Chloride 10
tr ans-1 ;2-Dich!oroethene 0.75
1. 1-Dichloroe\llane 0.25
2,2-Dich!oropropane 0.25
cis-1,2-Dichloioethcne 0.25
Chloroform 0.25
B,omochloromethane 0.75
1. 1.1-Trichloroethane 0.25
1, 1-0ichloropropene 0.25
Carbon Tetrachloride 0.75
1.2-Dichloroethane 0.25
Trich!oroethene 0.25
1,2-Dichloropropane 0.25
Bromodichlororne1hane 0.25
Dibromomethane 1
cis-1,3-0ichloropropene 0.25
\rans-1,3-Dichloropropene 0.25
1, 1,2-Trichloroethane 0,25
Telrachloroe\hene 0.25
1,3-Dichloropropane 0.25
Oibromochlorome\hane 0.75
1.2-Dibromoethane 1
Ch!orobenzene 0.25
1, 1.1,2-Tetrachloroelhane 0,25
Bromoform 0.5
1, 1.2,2-Tetrach!oroethane 0.75
Target Ouanlit;::itior1 limit-Subject 10
change due to instrument sensitivity
fentalively Identified. not confirmed
Estimated Value
Samples analyzed lor this compound but not detected
Sample not analyzed for this compound
Detected below quanlilalion limit
GC/MS Analysis performed
EHNR/DWQ LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 96-18-4 1.2,3-Trichloropropane
u 108-86-1 Bromobenzene
u 95-49-8 2-Chlorotoluene
0.59 106-43-4 4-Chlorotoluene
u 541-73-1 1,3-Dichlorobenzene
1.3 E 106-46-7 1,4-Dichlorobenzene
u 95-50-1 1,2-Dichlorobenzene
u 96-12-8 1, 2-Dibromo-3-Chloropropane
u 120-82-1 ·1 ,2,4-Trichlorobenzene
u 87-68-3 Hexachlorobuladiene
u 87-61-6 1.2.3-Trichlorobenzene
u 1634-04-4 Methy1-tert-bulyl ether
u 71-43-2 Benzene
u 108-88-3 Toluene
u 100-41-4 Ethyl benzene
u 108-38-3 m,p-Xylenes
u 95-4 7-6 a-Xylene
u 100-42-5 Styrene
u 98-82-8 lsopropylbenzene
u 103-65-1 n-Propylbenzene
u 108-67-8 1,3,5-Trimethylbenzene
u 98-06-6 tert-Butytbenzene
u 95-63-6 1,2,4-Trirnelhylbenzene
u 135-98-8 sec-Buty1benzene
u 99~87--6 p-isopropyltoluene
u 104-51-8 n-Bulylbenzene
u 91-20-3 Naphthalene
Gasoline Range Esti111ated Total Petroleum Hydrocarbon
Other purgeables detected
(up to 10 highest peaks)
NO VOLATILE ORGANIC COMPOUNDS
DETECTED BY GC/PID.
LAB NO. 7G0781
SUPERVISOR~
DATE~
ENlEREO BY . ·_:-::,
DATE . :_., ,
0.25 u
1 u
0.25 u
0.25 u
0.25 u
0.25 u
0.25 u
u
0.25 u
0.25 u
0.75 u
5 u
u
u
1 u
2 u
u
u
u
u
u
u
u
u
u
u
u
1119/l. rngll
D 25 N
Detected
ug/L
Nn~th Carolina Department of tnvironment, Health, , Natural Resources
D~vision of tpidamiology
Occupat.ional & Environmental Epidemiology Section
Drinkirx; llatar Health Jliak tvaluation
General -/ /,
/ DATE £/th,
(J Baaed on th••• analytical
for normal u1age.
-----"-h'-=/1.UL,U.,'-=-'-_ COUNTY
U\BOR.A'l'ORY 1iUMBE.R _'7....;_;_t;:_()1_/'.t_1 __
re1ult1, thi1 water ahoold bo con1id•r•d aaf•
( ) Chemical analysis did not ah0',1 any contamination. Water ahould be
reiampled if odor or taste .per1i1t,.
( ) The water should not be used for drinking or cooking purpo1es, avoid
prolonged bathing/showering.
( ) Baaed on .these analytical results, this water is highly contlllllinated and
should not be u1ed for drinking, cooking or bathing/showering.
( ) .The laboratory results are not conclusive, pleue reaample:
PLEASE INDICATE ON LAB SHUT THAT IT IS A R.ESAJo!PLE AND PROVIDE PREVIOUS
Skl-\PLE Nw.BE.R Is) .
( X) COHY.EITT'S:
The nitrate drinking water standard is 10 ppm. The nitrate level in your well
is below the drinking water standard. Continued consumption should no.t pose
any increased health risk based. on these nitrate levels.
For further infoI'!!\!ltion, contact Dr. Ken Ru6o, Occupat:i.onal and
Environmental Epidemiolcxn Section, [phone] or (919) 715-61,30.
DEHHR 3891 (5/92)
Environme~tol Epio8':'.ioloqy Sec:ion IRevi•w 5/95)
C0UN f"Y
QUAD NO:
IHEOELL
IU0!'1Jll.1' !O
COl I.EC I OR(S)
[),\ IE:
_,t_H_I_> _________ Rq:ional Office
lJ,\IILEN
418/97
11.\11:
f>URl'0SE:
LAIJOIUTOllY ANALYSIS
IJOlJJI0
COD I h~h 340
CUU Low 3)5
Colifom1: MffecalJ!616
Coliform MFTotalJ!504
IOC
! urbitity
Re5idue., Suspended SJO
1 ,,1al .Suspcn,kd w!ids
pH
All..alinit1· to pH 4.5
-\1\..alini!y to pll S.J
Carbonate
Bicarbonate
Carbon dio.~ide
Chluridc
Ch,,;,miurn· lk~ IUJ:!
Color: ·11 ue 80
C) ani<lc 710
C0,\1.\1[,''1'5:
111:UL
1ngtL
m;u'L
/JOOml
/lOOm!
mg/I
Nl"U
mg/L
rn;u'L
units
rng/L
in;u'L
m)?IL
mg.IL
mg/L
111,!VL
U)l,IL
rn
mg.IL
Owner:
Location or Sile
0escriptio11 of sampling poi111
Sampling Method·
Renmrks
Diss. Solids 70300
Fluoride 1)5 I
I lardness: total 900
Hardness: (non-earb) 902
Phenols J27JO
Spcdfic Cond. 95
Sulfate
Sulfide HS
Ml3AS
Oil and Grease
Silica
Boron
Formaldch,·de
NIB as N 610
TKN as N 625
' N02 +N0J as n 630
I': Tot~I as I' 665
1'0-t
llIVISION OF WATER QUALITY
Chemilll"}' L11l,or11lory Hqrnrl / Ground \V11"r Quality
SAMPLE PRIORITY
E]ROUTINE
EJ CHAIN Of CUSTODY
EJ SM11'LETYPE
rllYLI.IS FRYE WELi.
mg.fl
m~/L
mg.IL
m&'L
"&'L
u1'1hoYcm2
mg.IL
ni;;/L
mglL
mg.IL
mg/L
mg.IL
0.01 mg.IL
m5/L
5.2 mgtL
mglL
1ngll.
OE1'1ERGENCY
□
AB·Sil"er 46566
,\1.,,1111nin111l1 4[,557
As·Arsenic 46551
Ua-[Jruium 465511
Cn-Calciurn 46552
Cd-Cadium 46S59
Cr-Chromium 46560
Cu-Copper I 0~2
Fe-lion JQ..15 .
' Hg-Mercury 71900
K-l'olassium 46555
Mg-1,1:ignesium '127
1'ln-l,langa11ese 1055
Na-Sodium 929
Ni-Nid.cl
Pb-lead ~6564
Sc-Selenium
Zn Zinc ~6567 -
•
Lab Number 7G0797
Dale Received · ~l'n97
Time Recei, cd 9:30AM
Rccci,cd By DS
Released Br OS
Dale rcpor1cd: SIi 3197
ug/L Ori;anochlorine Pesticides
1,),(11. I hi,i'""'l'h"~l'lu>111~ r•c~ucidn
ugll. Niu,,gen l'cs1icides
ug/L
m,!VL Acid lkrllicodcs
u;u'I.
ug/L Semi,ola!iles
ugfl. 11'1 !-Diesel R:111ge
uglL
2.5 ugll. ' \"ob1ile 0,ganics (\"0,\ honk)
mgll.
mg·L J"!'I I-Gasoline Range
ugll. l"l'I 1-U I EX Gasoliue Range
mg'L
ug1L
uglL
ug.'L
uglL '
7G0797APR
I, .. '.
GROUNDWATER FIELD/LAB FORM
North Carolina
Department ol Envlronmenl, Heallh, and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
County Jrv&-C/
Quad No Ll 7 Y/ cj
Lat."3.:r"'f.:1/ S7:;'''N
SAMPLE TYPE SAMPLE PRIORITY Lab Number __ ,.J,..c.,,,.,1-,,J...,,'-L....'--J.-.----,,,--c'c---
Serial No. _______ _
~-_,_,c; ,·-<->,,., e ''W Long. C2:!_ Y L> 1
Report To: ARO, FRO, MBO/ ARO, WaRO, WiRO,
Ei Water :i:J.Routine
0 Soil O Emergency 0 Other ________ _
;gl Chain of Custody
WSRO, Kinston FO, Fed. Trust, Central 011., Other: ________ _
Shipped by: Bus,~i;?, Hand Del., Other_· ____________ _
Dale Received ..'.:Ll.....!~-l-'-0 Other: __________________ _
Data Entry By:, ______ Ck: ______ _
Date Reported: ______________ _
~~ I . ~•=e Colleclorjs): J/c,h I e.,., Dale 'f 2/51 Time Ii· I) Baseline, Complaint, Compliance, LUST.Pesticide Siudy, Federal Trust, Other:
FIELD ANALYSES --;71 / · -(c11cloooe) , "/(. Owner n,!J /tJ . rr'JE' Ueq ('1;:,,11-<Rcl] R,·,t,, I f,u.,.., uc 11)
pl-1400 ,,., f, .u Spec. Cond.94 I J;'6 at,25-0 C Location or site _.uc,<';;~,_..L.w..,;:.e,,~=_:. __________________________ _
Temp.10 · °Cf . Odor Descripti_on ol sampling point _..c,ccu=i'-"--"-''"-'1,,' _______________________ _
Appearance GI ec:,:-,c
1
c/c,-G,_rs Sampling Method ---------',0-e,_,_"-.,-~--•-"--'--------Sample Interval ________ _
Field Analysis By: -~u~c:.~-~-'&.,,.,=----------Remarks _.ti..L__,1:..,·=~~=_.,=~'-----'~'-----------------------------
LABORA TORY ANALYSES "'""''"''"''·"'"="'""'
BOD 310 mail Diss. Solids 70300 rnn/1 l An -Silver 46566 un/1 Organochlorine Peslicides
COO Higl1 340 mg/I Flouride 951 mo/I I Al -Aluminum 46557 un/1 O•ganoohosphorus Pesticides -· COD Low 335 m9~ Hardness: Total 900 rnn/1 i As -A1senic 46551 un/1 Nitroaen Pesticides
ColHorm: MF Fecal 31616 1100ml Hardness lnon-carbl 902 mn/1 Ba -Barium 46558 un/1 Acid Herbicides
Colilorm: MF Total 31504 /1001111 Phenols 32730 ug/1 Ca -Calcium 46552 mn/! PCB's
TOC 680 ma/I Soec1flc Con\;1. ~;! uMhQS;[!;;:rn~ Cd -Cadmium 46559 un/1
Turbidity 76 NTU Sullale 945 mn/1 Cr -Chromium 46560 un/1
Residue., Suspended 530 mg/I Sullide 745 mo/I Cu -Conner 46562 un/1
Fe -Iron 46563 ua/1 Semivolatile Organics
Oil and Grease ma/I X Hg -Mercury 71900 ug/1 TPH -Dlesel Range
pH ,,03 unit~ K -Potassium 46555 rng/1
Alkalinity lo pH 4.5 410 mg/I Mg -Magnesium 46554 mq/1
Alkali11ily lo pH 8.3 415 mg/l Mn -Monnanesc 46565 un/1
Carbonate 445 mg/I NH ·asN 610 rnn/1 Na -Sodium 46~56 nm/I I-:;:? Volatile Organics (VOA bollle)
Oicarbonale 440 mg/I I~~ as t:J 625 moll "'; -'"''·~' -" TPH -Gasoline Ranoe
Cacbon dioxide 405 mg/I >< NO. + NO as N 630 rnn/1 Pb -Lead 46564 un/1 TPH -BTEX Gasollre Range
Chloride 940 rng/1 P: T olal as P 665 rnn/1 Se -Selenium uo/1
Cllrornturn: Hex 1032 ug/1 Zn -Zinc 46567 un/1
Color: True ao cu
Cyanide 720 mg/I
Lab Comments:--------------------------------------------------------------
GW-5-1 nEV. 7/' For Dissolved Analysis -submit filtered sample and wrile "DIS" in blc
EHNR/DWQ LABORATORY LAB NO. 7G0797
~k_ VOLATILE ANALYTICAL REPORT
REPORTED BY SUPERVISOR "J<el<
CHECKED BY DATE ,-p· u
REVIEWED BY _ t¼J,,
ENTERED BY
SAMPLE TYPE: WATER ANALYSIS RESULTS DATE C,
75-35-<1 1.1-0ichloroelhene 0.75 u 96-18-4 1.2.3-TriC:hloropropane 0.25 u
75-09-2 Methytene Chloride 10 u 108-86-1 Bromobenzene 1 u
156-60-5 trans-1,2-Dichloroelhene 0.75 u 95-49-8 2-Chlorotoluene 0.25 u
75-34-3 1.1-Dichloroelhane 0.25 0.59 106-43-4 4-Chlorotoluene 0.25 u
590-20-7 2.2-Dichloropropane 0.25 u 541-73-1 1.3-0ichlorobenzene 0.25 u
156-59-4 cis-1.2-Dichloroethene 0.25 0.46 106-46-7 1,4-0ichlorobenzene 0.25 0.71
67-66-3 Chloroform · 0.25 39 E 95-50-1 1,2-Dichlorobenzene 0.25 u
74-97-5 Bromochlorome\hane 0.75 u 96-12-8 1, 2-0ibromo-3-Chloropropane 1 u
71-55-6 1, 1, 1-Trichloroethane 0.25 u 120-82-1 1.2.4-Trichlorobenzene 0.25 u
563-58-6 1. 1-Dichloropropene 0.25 u 87-68-3 Hexaclllorobuladiene 0.25 u
56-23-5 Carbon Tetrachloride 0.75 u 87-61-6 1,2,3-Trichlorobenz~ne 0.75 u
107 -06-2 1.2-Dich/oroelhane 0.25 u 1634-04-4 Melhyl-tert-butyl ether 5 u
79-01-6 T rich!oroethene 0.25 u 71-43-2 Benzene u
78-87-5 1.2-Dichloropropane 0.25 u 108-88-3 Toluene u
75-27-4 8romodic!1loro1nel11ane 0.25 3.0 100-41-4 Ethyl benzene u
74-95-3 Dibromornethane u 108-38-3 m,p-Xylenes 2 D
10061-01-5 cis-1,3-0ichloropropene 0.25 u 95-47-G o-Xy!ene 1 u
10061-02-6 !1 ans-1,3-0ichloropropene 0.25 u 100-42-5 Styrene u
79-00-5 1. 1,2-Trichloroethane 0.25 u 98-82-8 lsopropylbenzene u
127-18-4 Telrachloroelhene 0.25 u 103-65-1 n-Propy!benzene u
142-28-9 1,3-Dichloropropane 0.25 u 108-67-8 1,3,5-T rimelhylbenzene u
f24-48-1 Oibromochloromethane 0.75 1.0 98-06-6 tert-Butylbenzene u
106-93-4 I. 2-Dibromoethane u 95-63-6 1.2, 4-T,imethylbenzene u
108-90-7 Chlorobenzene 0.25 u 135-98-8 sec-Butyl benzene u
630-20-6 1, 1. 1.2-Telrachloroelhane 0.25 u 99-87-6 p-isopropylloluene u
75-25-2 Bromoform 0.5 u 104-51-8 n-Bulylbenzene u
79-34-5 1.1,2,2-Tetrachloroelhane 0.75 u 91-20-3 Naphthalene u
mg/L mgll
l OL-Target Ouantitalion Limit• Subject lo Gasoline Range Estimated To!al Petroleum Hydroca1bon O 25 N
change due lo instrument sensitivity
T-Tentatively !denlifted, not confirmed Other pur9eables detected Detected
E-Estimated Value (up to 10 highest peaks) ugll
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound
0-Detected below quantila\ion limit
M-GC/MS Analysis performed
COMMENTS
' ,, I
State of North Carolina
Department of Environment,
Health and Natural Resources
Mooresville Regional Office
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
AVA
DEHNR
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
A.A.A. Enterprises, Inc.
DIVISION OF WATER QUALITY
May 28, 1997
% Henry Sigmon -Registered Agent
248 Mitchell Trail
Statesville, North Carolina 28677
Dear Mr. Sigmon:
RE: Notice of Violation
15A NCAC 2L Classifications and
Water Quality Standards Applicable
to the Groundwaters
Sigmon Septic Tank Service
Groundwater Incident N° 3422
Priority Rank 205A
Class AB
Iredell County, N.C.
I.O _,
:JI: =<
N
O">
Chapter 143, North Carolina General Statutes, authorizes and
directs the Environmental Management Commission of the Department
of Environment, Health, and Natural Resources to protect and
preserve the water and air resources of the State. The Division
of Water Quality has the delegated authority to enforce adopted
pollution control rules. This letter is a standard notification
and is intended to advise you of the legal requirements under
North Carolina law.
Specific violations of 15A NCAC 2L .0103(d) -No person
shall conduct or cause to be conducted any activity which causes
the concentration of any substance to exceed that specified in
15A NCAC 2L .0202 -are as follows:
Constituent (183 Lauren Drive) Concentration* 2L Standard*
mercury
*Concentration in parts per billion
919 North Main Street,
Mooresville, North Carolina 28115
Voice 704-663-1699
2.5 1 . 1
FAX [phone]
An Equal Opportunity/ Affirmative Action Employer
50% recycled/lO"k post-consumer paper
A.A.A. Enterprises, Inc.
May 28, 1997
Page Two
You are responsible for causing, contributing to or allowing
the continuing violation of the underground water quality
standards because you stored and/or disposed of septage waste in
unlined lagoons on the property from which the contamination
originates.
15A NCAC 2L .0106(b) states that any person conducting or
controlling an activity which results in the discharge of a
waste, hazardous substance or oil to the groundwater, or in
proximity thereto, shall take immediate action to terminate and
control the discharge, mitigate any hazards resulting from
exposure to the pollutants and notify the Department of the
discharge.
To comply with this section of the rules, you must provide
an alternate drinking water supply for the residents who use the
well at 183 Lauren Drive, Statesville, within seven days of
receipt of this letter.
You should be aware that any violation of 15A NCAC 2L may
subject you to a civil penalty assessment under the authority of
G.S. 143-215.6A of up to $10,000 per rule violation. Each day
that the violation continues may be considered a separate
violation. Failure to respond within the time specified and to
voluntarily achieve compliance may result in a recommendation for
enforcement, the issuance of a Special Order against you under
the authority of G.S. 143-215.2, or a request to the Attorney
General to institute an action for injunctive relief.
Your response and/or questions should be directed to Paul
Dahlen of the Mooresville Regional Office at [phone], ext.
234.
cc:
D. Rex Gleason, P.E.
Acting Regional Supervisor
JTed Bush -Central Office
Jesse Wells -Hazardous Waste
Iredell County Health Dept.
Enclosure: Health Risk Assessment -183 Lauren Drive
\prd\sigmon.nov
COUNTY
QUAD NO:
97Mf1Yilf flllll:20
IREUELL
REPORT TO _,_1_R00 _________ Rcgional omcc
COLLECTOR(S) : c"c"='=' L=E="e-,--------
DATE: 418197
TIME:
PURPOSE·
LABORATORY ANALYSIS
BOD JIO
COD lligh 340
COD LowJJS
Colifmrn· MFFccal31616
Coliform: MF Total 31504
TOC
Turbitity
Residue, Suspended 5J0
roral Suspended solids
pl!
Alkalinity to pH 4.5
Alkalinity ID pH 8,3
Carbonate
Bicarbonate
Carbon dioxide
Chloride
Chro1nium: Ile" 1032
Color: True 80
Cyanide 720
CO/\IMENIS:
mg/L
mg/I.
mg/L
1100ml
/1001111
mgil
NTU
mg/L
msfL
units
mg/L
mglL
mg/L
mg/L
mg/L
rng/L
,g!L
C.U.
mglL
Ov.ner:
Location or Si1e:
Uesc,iption of san,pling point
Sampling l\1cthod·
Remarks·
Diss. Solids 70300
Fluoride '151
Hardness: total 900
Hmdness: (non-carb) 902
Phenols 327J0
Spccilic Cond 95
Sulfate
Sullide 745
MBAS
Oil'1IldGmm
Silica
lloron
Formaldehyde
Nl\3 as N 610
lKNasN625
' NO2 +NOJ as n 630
I': ·101at as P 665
l'O.J
DIVISION OF WATER QUALIT\'
Chcmistr-y l.•bor11lory Rtporl / Ground Watu Qu1li1y
SAMPLE PRIORITY
E)ROUTINE
E] CIIAINOFCUSTODY
@J SAMPLE TYPE
1'11"1"1.LIS FRYE \\'ELI.
mg/L
lllflll.
mg/L
mg/L
,g!L
ulllhoslcm2
mg/L
mg/L
mgll,
mgll.
mg/L
mg/L
0.01 mg/L
mg/I.
5.2 mglL
rnglL
mg!L
□EMERGENCY
□
Ag-Silver 46566
AI-Al11111i11um 4C,557
As-Arsenic 46551
lla-Unrium 46558
Cn-Cakium 46552
Cd-Cadium 4655'1
Cr-Chromium 46560
Cu-Copp!.'• 1042
Fe· Iron 1045
' Ilg-lllercury 719()()
K-l'otassium -16555
Mg-111agnesiu111 '127
Mn-111:mgancse 1055
Na-Sodium 929
Ni-Nid.cl
Pb-Lead -1656-1
Sc-Selenium
Zn Zinc 4656 7
2.5
Lab Number 7G0797
lJate Recci~·cd 419/97
Time Rccci, ed 9:30 AM
Rccci.,:d By us
Released By DS
Date 1eponed : SIIJ/97
ug/L Organochlo,inc Pesticides
UJj.ll. l l1i::mn1,hn•1~,u1u~ l'c~1icitk'I:
ugll. Nmogcn Pesticides
ug/L
m!l,.IL Acid flcrbicidcs
ug/L
ui;/L Scmi,olatilcs
ug/L l'l'll-ll1cscl Rm1ge
U!!-'L
ugll. ' Volatile U,gamcs (\'O,\ bonlc)
mgll.
mg•L l"PII-Gasolinc Range
ug/L rrl 1-IJTEX liasolinc Ran!:C
mg'L
ug1L
ug,L
ug1L
ug1L
1G0191 APR
-Norlh Carolina
GROUNDWATER FIELD/LAB FORM Department ol Environment, Health, and Natural Resources
DIVISION OF WATER QUALITY· GROUNDWATER SECTION
County ,krG,ciL(d
Quad No LL 7 n 8
Lat.3,:(" 'I ;z' S?;'''l\J
Serial No. ______ _
c,.,.-,0,•-w/ e''ILJ Long. [2,/_ 0 '--' 1
Report To: ARO, FRO, Moo/ RRO, WaRO, WiRO,
SAMPLE TYPE
fl water D Soil
D Other
SAMPLE PRIORITY
:t::3-Routine
D Emergency
----------
:Es] Chain of Custody
WSRO, Kinston FO, Fed. Trust, Central Off., Other: ________ _
Shipped by: Bus,~i~, Hand Del., Other· ____________ _
0 Data Entry By: _______ Ck: _______ _
Date Reported: ______________ _
""-~ t ( . Purpose:
Collector(s): J/c:,h I en Date 'f 2, 71 Time It· 1) Baseline, Complain!, Compliance, LUST, Peslicide Sludy, Federal Trusl, Oiher: __ _ __ tc11clo ooeJ ,
FIELD ANALYSES /1.. Owner ?l'!J(l!J . ,-,-')'! Welj C6,,n-<Rc ''.J i<\ d,. I L~u .... , , >,; 1<)
pH400 "'--(, .v Spec. Cond.94 / j'o at-25" C Location or site c:~ W-
Temp.10 · 0c . Odor_______ Description of sampling point -==·l=s"-'---"-"",_._· ______________________ _
Appearance G ( e.c.r,fC < / c;.,-G,___rs Sampling Method ,;;::::i_._ Sample Interval \ I --------,~-~~,-'-½-,-,.,-,-"~,-----------------
Field Analysis By: -~V~~=~~-e.,,.,=---------Remarks -Ll...'--''-'·=1-~=-"""'""-------------------------------
LABORA TORY ANALYSES (p"''''"''""'·'""""'·'"·'
BOD 310 ma/I Diss. Solids 70300 ma/I . I Ao -Silver 46566 ua/1 Organochlorine Pesticides
COD High 340 mg/I Flouride 951 mail l Al -Aluminum 46557 uq/1 O•ganophosphorus Peslicides -· COD Low 335 rng/1 Hardness: Tolal 900 rnn/1 i As -A1 senic 46551 ua/1 Nitroqen Pesticides
Colilorm: MF Fecal 31616 1100ml Hardness lnon-carb} 902 mn/1 Ba -Barium 46558 ua/1 Acid Herbicides
Coliform: MF Toial 31504 /100ml Phenols 32730 ug/1 Ca -Calcium 46552 lll(J/1 PCB's .
TOG 680 ma/I SR~QifiQ CQnQ. ~~ uMhQ~[Qrn~ Cd -Cadmium 46559 un/1
Turbidily 76 NTU Sullale 945 mo/I Cr -Chromium 46560 ua/1
Residue., Suspended 530 mg/I Sullide 745 mall Cu -Conner 46562 uq/1
Fe -· Iron 46563 ug/1 Semivolalile Organics
Oil and Grease mall X Hg -Mercury 71900 ug/1 TPH • Diesel Range
pH 403 unil~ K -Polassium 46555 mg/!
Alkali11ily to pH 4.5 410 mg/I Mq -Maqnesium 46554 mq/1
Alkalinily lo pH 8.3 415 mg/I Mn -Manoanese 46565 ua/1
Carbonate 445 mg/I NH as N 610 ma/I Na -Sodium 46~56 mq/1 x Volalile Orga11ics (VOA bollle)
Bicarbonate 440 mall I TKN "" N coc "'"" .i; -•1;ekol "n/1 TPH -Gasollne Ranae
Carbon dioxide 405 mg/I X NO~ + NOa as N 630 mg/I Pb • Lead 46564 ua/1 TPH -BTEX Gasollre Range
Chloride 940 mg/I P: Tola! as P 665 ma/I Se -Selenium uq/1
Chromium: Hex 1032 ug/1 Zn -Zinc 46567 uo/1
Color: True 80 cu
Cyanide 720 mg/I
Lab Comments:-----------------------------------~----------------------
GW-54 REV. 71' For Dissolved Analysis -subrnil filtered sample and wrile "DIS" in bl<
EHNR/DWQ LABORATORY LAB NO. 7G0797
~ VOLATILE ANALYTICAL REPORT
REPORTED BY SUPERVISOR 'K,C.
CHECKED BY DATE t5 t:J·
REVIEWED BY t¼J,,
ENfERED BY J
SAMPLE TYPE WATER ANALYSIS RESULTS DATE
75.35.4 1, 1-Dichloroethene 0.75 u 96•18·4 1,2, 3-l richloropropane 0.25 u
75-09-2 Melhylene Chloride 10 u 108-86-1 Bromobenzene 1 u
156-60-5 trans-1,2-0ichloroethene 0.75 u 95-49-8 2-Chlorotoluene 0 25 u
75-34-3 1, 1 •0ichloroethane 0.25 0.59 106-43-4 4-Chlorotoluene 0.25 u 590-20•7 2,2-Dichloropropane 0.25 u 541-73-1 1.3-0ich!orobenzene 0.25 u
156-59-4 cis-1.2-0ichloroethene 0.25 0.46 106-46-7 1,4-Dichlorobenzene 0.25 0.71
67-66-3 Chloroform 0.25 39 E 95-50-1 1,2-Dichlorobenzene 0.25 u
74-97-5 Bromochloromethane 0.75 u 96-12-8 1, 2· Dibromo-3-C hloropropane u
71-55-6 1, 1, 1-Trichloroethane 0.25 u 120-82-1 1.2,4-Trichlorobenzene 0.25 u 563-58-6 1, 1 •Dichloropropene 0.25 u 87-68-3 Hexachlorobutadiene 0.25 u
56-23-5 Carbon Tetrachloride 0.75 u 87-61-6 1,2,3-Trichlorobenzene 0.75 u
107-06-2 1,2-Dichloroethane 0.25 u 1634-04-4 Melhyl-tert-bu\yl ether 5 u
79-01-6 T richtoroe\hene 0.25 u 71-43-2 Benzene 1 u
78-87-5 1.2-Dichloropropane 0.25 u 108-88-3 Toluene u
75-27-4 Bromodichloromelhane 0.25 3.0 100-41-4 Ethyl benzene 1 u
74.95.3 Dibromomethane u 108-38-3 m,p-Xylenes 2 0
10061-01-5 cis-1,3-Dichloropropene 0.25 u 95-47-6 a-Xylene u
10061-02-6 trans-1,3-Dichloropropene 0.25 u 100-42-5 Styrene u
79-00•5 1, 1,2-Trichloroethane 0.25 u 98-82-8 lsopropylbenzene u
127•18-4 Tetrachloroethene 0.25 u 103-65-1 n-Propylbenzene u
142-28-9 1,3-Dichloropropane 0.25 u 108-67-8 1,3,5-Trimethylbenzene u
124-48·1 Dibromochloromethane 0.75 1.0 98-06-6 tert-Butylbenzene u
106-93-4 1.2-Dibromoethane 1 u 95-63-6 1,2,4-T rimethylbenzene u
108-90-7 Ch!o·robenzene 0.25 u 135-98-8 sec-Butyl benzene u
630-20-6 1, 1, 1,2-Telrachloroethane 0.25 u 99-87-6 p-isopropyltoluene u
75-25-2 Bromoform 0.5 u 104-51-8 n-Butylbenzene u
79-34-5 1, 1,2,2-Tetrachloroelhane 0.75 u 91-20-3 Naphthalene u
rng/L mgll
TQL-Target Quanli\ation Limit-Subject to Gasoline Range Estimated Total Petroleum Hydrocarbon 0 25 N
change due to instrument sensitivity
T-Tentatively Identified. not confirmed Other purgeables detected Oetec\ed
E-Estimated Value (up to 10 highest peaks) ug/L
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound
0-Detected below quanlilation limit
M-GC/MS Analysis performed
COMMENTS;
-
COUNTY
QUAD NO:
IREOELL
q~.,,v I' .. J i H: I l J P111=28
REPORT TO J\IRO
COLLECTOR{S) UAIILEN
cc=~-------Regional Office
DATE: 4n/97
TIME:
PURPOSE:
LABORATORY ANALYSIS
UOO JIO
COO I ligh 340
COD Low JJS
Coliform: MF Fecal 31616
Coliform: /.IFTotalJl504
lOC
Turbitily
Residue., Suspended SJO
Toca! Suspended solids
pll
Alkalinity to pl I 4.5
Alkalinity lo pll 8.J
Carbonate
Bicarbonale
Cmbon dio . .cide
Chloride
Chromium: lk.c 1032
Color: True 80
C}anide 720
COMMENTS:
mg/L
m!!fl
m&'L
1100ml
1100ml
mg/1
NTU
mg/L
mg/L
units
mg/L
mg/L
mg/L
m!;IL
mg/L
mg/L
ug/L
'"
mg/L
Owner:
Loc:ition or Si1c·
Description ofsamplin!! point
Sampling Method:
Rcm;uks·
Oiss. Solids 70100
l'!uoride 951
I lardncss: total 900
11:udness: (non-carb) 902
Phenols 32730
Specific Cond. 95
Sulfate
Sulfide 745
MBAS .
Oil and Grease
Silica
Boron
Formaldeh)·de
NHJ as N 610
rKN as N 625
X N02 +N03 as n 630
P: Total as P 665
1'04
UIVISJON OF WATER QUALITY
ChcrniJhJ' L11l111r111Dr)' Report/ Grou11d Water Quality
SAMPLE PRIORITY
~ROUTINE
BJ CIIAIN OF CUSTODY
(EJ SAMPLE TYPE
,\LLEN CASCADIJEN
m&'L
mglL
mg1L
mg/L
,g/L
u1\1hoskm2
mgfL
mg/L
mg.IL
mg/L
mg/L
,nglL
0.01 m51L
. mg.IL
12 111gll.
<0.01 mg/L
mg/L
□E/'.IERGENCY
□
Ag-Sihcr 4656(,
,\1-,\luminum 46557
As-A,senic 46551
Ba-Barium 46558
Ca-Cakium 46552
Cd-Cadium 46559
Cr-Chromium 46S60
C'u-Copper 1042
Fe-hon 1045
X Ilg-/llcrcu,y 71900
K-l'otassium 46555
Mg-Magnesium 927
r,.1n-/llanga11cse 1055
Na-Sodium 919
Ni-Niclel
!'b-Lcad 46564
Sc-Sc!cnirnn
Zn_Zinc46567
lab Numbc, 7GU781
Dale Recei, cd 4/8197
Time Rccci, ed '1.00AM
R,m:i,cd Uy OS
Released Br OS
Da!c repo1lcd · 5/1Jr9J
uglL O,ganuchlrnine l'c~1icides
u!l)L Org;snophusphotus Pesticides
ug.il. N11ro!_:en Pesticides
ug•I.
mglL Aciil I krbicides
ugiL
ug1L Sen1i, ulaliks
uglL 11'1 I-Uiescl R311ge
ugiL
I. 1 ug/1. X \'ola1ilc Organics (\"0,\ bottle)
mg1L
,ngll I l'I 1-Gawline Range
ug/L 1"1'11-B 1 EX Gawline Range
mglL
ug1L
ui:;IL
ug1L
ug'L
1G01!1 APR
North. Cn1oll11a
GROUNDWATER FIELD/LAB FORM . Department of Envlronrncnl, lfcallh, and Nalural Resources
'. :'. _\' ,) )llVISION OF ENVlnONMENTAL MAf!AGEMENT-GnOUfJDWATEn SECTIOJJ
County L-:u:l, ,li
Quad No L(,7 "t Serial No. ______ _
Lat. 35 ~ 4 L' .s·"2-'"NLong. /?o O ~--;7i 11 ~ u
. -·-:-, '
Report To: ARO, FRO,~RRO, WaRO, WiRO,
SAMPLE PRIORITY
[:2lnoUTINE □EMERGENCY
•. BJcHAIN OF CUSTODY
WSRO, Kinston F9, ~-Trust, Central Off., OIiier:
Shipped by: Bus.~. Hand Del., Otl1er·--c -~----------
0
Lab Number --"M"= D_'i]Z_\ -7"'c-c:c=,sc---
Date Received -\:t::[_ Time ..=l:-'-"'-'="'-----
nec·d by:_ From: Bu. oui, . Hand Del.,
Other: _________________ _
Data Entry By: ______ Ck: ______ _
Date Reported: _____________ _
Collector(s):. ye b,( <6n Date q'"/ f7 l.rw ,_,,,"' )'j.l.2..
Purpose:
Time ~/~}_-'_",_-I~(.,~_ Baseline, Complaint, Compliance, LUST, Peslicide Study, Federal Trust, Other: ,c11cl& OIMI) FIELD ANALYSES Owner ,&l" o (Gr<.; cl,! ~
pi-1 400 s-::-..s: J-Spec. Cond.94 /l o at~C Location or site _...."""'"'-_,_-'--'---(_=c:,_,,_."-'-'~-"i ec•+•=...,....,__-"'-'-"'-,=='-'(""L,._-_____________ _
Temp.10 • 0 c Odor ______ _
Appearance ,, C""'--/-::,,., /;-{.,,__µ·
Description or sampling point -4"'7'"----'~"----'"'='"""·"""~,__,c.."'f='--'--""'-'--"--""---------------
Field Analysis By: __ '.-1)~,;:-h~,~te,,~-------
LABORATORY ANALYSES
Sampling Method -------+~=.....,~-~~-------Sample Interval _______ _
~b.11101, o!c) nernarks I ..-<.. ~
(purnpinq lime, air temp. elc.)
BOD, 310 rng/I Diss. Solids 70300 mq/1 Ag • Silver 46566 ug/1 O1ganocl1fmine Pesticides --
COD High 340 mg/I Flouride 951 mq/1 /\I -Alu111inurn 4G557 · uqll Organophosphorus l1esticides --COD Low 335 mgil Hardness: Total 900 mgll As -Arsenic 46551 ug/1 Nitrogen Peslicides
Colilorm: MF Fecal 31616 1100ml Hardness (non-cmb) 902 mg{!_ 0a -Barium 46558 ug/I --
Coliform: MF Total 31504 /100ml Phenols 32730 ug/1 Ca -Calcium 46552 mg/I /\cid He,bicides
TOG 680 mg/I ___S__gecilic Cond. 95 uMhos/cm2 Cd -Cadmium 46559 ug/1 --
Turbidity 76 NTU Sullate 945 m~I Cr -Chromium 46560 ugil Se111ivolatile Organics
Residue., Suspended 530 mgtl Sullide 745 111911 Cu -Co~eer 46562 ·ug/I
Fe -hon 46563 ugtl x ~ Hg -Me1cu1y 71900 ugil Volatile Organics (VOA l>olllt.?)
pH 403 units K -Potassium 46555 mg/I
Alkalinity lo pH 4.5 41D mg/I Mg -Magnesium 46554 mg/I TPH -Gasoline nange
Alkalinity to pH 8.3 415 mg/I Mn -Manganese 46565 u9!I TPH · B1 EX Gasoline Range
Carbonate 445 mgil NH, as N 610 mg/I Na -Sodium 46556 mg/I
Bicarbonate 440 mg/l --TKN as N ..52s 1111)1]. Ni· Nickel ug/1
Carbon dioxide 405 mgil ,.....__,., NO + NO, as N 630 mgtl Pb · Lead 46564 ug/1 I
Chloride 940 mg/I P: Total as P 665 1119/I Se -Selenium ug/I I/ --Chromium: Hex 1032 ug/I Zn -Zinc 46567 ug/I V
Color: True 80 Pt-Co
Cyanide 720 mg/I
Lab Comments:---------------------------------------------------------
GW-54 REV. &'93 For Dissolved Analysis -submit filtered sample and wrile "DIS" in block.
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE·
75-35-4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
106.-93-4
108-90-7
630-20-6
75-25-2
79-34-5
TQL-
T-
E-
U-
N-
0-
M-
COMMENTS:
WATER
1. 1-Dichloroethene 0.75
Methylene Chloride 10
trans-1,2-Dichloroethene 0.75
1, 1-Dichloroethane 0.25
2,2-Dichloropropane 0.25
cis-1,2-0ichtoroethene 0.25
Chloroform 0.25
Bromochtoromethane 0.75
1, 1, 1-Trichloroethane 0.25
1. 1-Dichloropropene 0.25
Carbon Tetrachloride 0.75
1. 2-Dichloroethane 0.25
Trichloroethene 0.25
1.2-Dichloropropane 0.25
Bromodichloromelhane 0.25
Dibromome\hane 1
cis-1,3-Dichloropropene 0.25
lrans-1,3-Dichloropropene 0.25
1, 1,2-Trichloroethane 0.25
T etrachloroethene 0.25
1,3-Dichloropropane 0.25
Dibromochloromethane 0.75
1.2-Dibromoethane
Chlorobenzene 0.25
1, 1, 1,2-Tetrachloroethane 0.25
Bromoform 0.5
1, 1,2,2-T etrachloroethane 0.75
Target Quanlitation Limit-Subject to
change due to instrument sensitivity
Tentatively Identified, not confirmed
Estimated Value
Samples analyzed for this compound but not detected
Sample not analyzed for this compound
De!ected below quanlilation limit
GC/MS Analysis performed
EHNR/DWQ LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 96-18-4 1.2,3-Trichloropropane
u 108-86-1 Bromobenzene
u 95-49-8 2-Chlorotoluene
0.59 106-43-4 4-Chlorotoluene
u 541-73-1 1.3-Dichlorobenzene
1.3 E 106-46-7 1,4-0ichlorobenzene
u 95-50-1 1,2-0ichlorobenzene
u 96-12-8 1,2-Dibromo-3-Chloropropane
u 120-82-1 1,2,4-T richlorobenzene
u 87-68-3 Hexach!orobutadiene
u 87-61-6 1,2,3-lrich!orobenzene
u 1634-04-4 Melhyt-tert-butyl elher
u 71-43-2 Benzene u 108-88-3 Toluene
u 100-41-4 Ethyl benzene
u 108-38-3 m,p-Xylenes
u 95-47-6 a-Xylene
u 100-42-5 Styrene
u 98-82-8 lsopropylbenzene
u 103-65-1 n-Propylbenzene
u 108-67-8 1.3.5-T rimethylbenzene
u 98-06-6 lert-Butylbenzene
u 95-63-6 1,2,4-Trimethylbenzene
u 135-98-8 sec-Butylbenzene
u 99-87-6 p-isopropylto1uene
u 104-51-8 n-Butylbenzene
u 91-20-3 Naphthalene
Gasoline Range Estimated Total Petroleum Hydrocarbon
Other purgeab!es detected
(up to 10 highest peaks)
NO VOLATILE ORGANIC COMPOUNDS
DETECTED BY GC/PID.
LAB NO. 7G0781
SUPERVISOR~
DATE~
EN'! ERED BY . . /
DATE ~-r
0.25 u
1 u
0.25 u
0,25 u
0.25 u
0.25 u
0.25 u
1 u
0.25 u
0.25 u
0.75 u
5 u u
u
I u
2 u
u
u
u
u
1 u
1 u
u
u
u
u
u
mg/l. mgll
0.25 N
Delecled
ug!L
COUNTY
QUAD NO
•H j 1 • 28 l·l! ! 1 •
REPORT TO
COLLECTOR($)
DATE:
c'c'c•co~~-------Regional O/fice
DAIil.EN
417197
TIME·
PURPOSE:
LABORATORY ANALYSIS
BOD 310
COD High 340
COD Low335
Coliform: MF Fecal 316!6
Coliform: MFTotal315Q.l
TOC
Turbitity
Residue .• Suspended 530
Total Suspended solids
pH
Alialini1y to pll -1.5
Alkalinity to pll 8.3
Carbonate
Bicaibonate
Carbon dioxide
Chlo,ide
Chromium: lk< IOJ2
Color: Troe 80
Cyanide 7:!0
CO/\IME/'HS:
mg.IL
mg/L
mg/L
1100ml
1100ml
mg/1
NTU
mg/L
mg/L
units
mglL
rng/L
mg/L
mglL
mg/L
mgiL
,~L
'" mg.II.
Location or Sile
Desc1iption of sampling p(iinl
Sampling Method
Remarks
Diss Solids 70JOO
Fluoride 951
Hardness: total 900
Hardness: (non-carb) 902
Phenols )2730
Spc,dfic Co11d. 95
Sulfate
Sulfide 745
MllAS
Oil ru,d G,ease
Silica
llomn
Formaldehyde
NIB as N 610
n~N as N 625
' NU2 +NOJ as n 630
1': Total as P 665
l'OJ
01\'ISION OF WATER QUALITY
MMPLE PRIORI rv
[]ROUTINE
~ CIIAIN OFCUSlOlJY
E:J SMll'l.E TYl'E
CIIIUS UA \'IUSON HES.
mg/L
mg/L
mg/L
mg/L
,giL
u1'1hos/cm2
mg/L
m;;IL
mg.IL
mg.IL
mg.IL
mg.IL
<0.01 mg.IL
mglL
1.4 mgiL
0.04 mglL
111~1.
DEJ'.1ERGENCY
□
,\g-Siher 46566
Al-Aluminum 46557
As-Arsenic 46551
Ba•llarium 46558
Ca.Calcium -165S2
Cd•Cadium 46559
Cr-Chromium 46560
Cu• Copper 1042
Fe· lrori 1045 ., Ilg• Mc1cury 71900
K-Potassium 46555
Mg· Mngncsiu111 <J:7
1'1n-1'1an£nncsc 1055
Na-Sodium 919
Ni-Nid.d
Pb-Lend J65(>.l
Se•Sclcuirnn
Zn_ Zinc J(,5(, 7
I.ab Number 7(.;0777
IJ;i1e Recci, ed -1111197
1 ime Recci, cd Q 00 A1'1
Recei,ed I!~ lJS
Rcle;,scd llv DS
1 hie ,cpor1c,I · 511.11•11
ugtl. O1ganochlorinc Pcs1icides
uglL Organophosphorus Pes!icidcs
uglL Ni!rogcn Pesticides
ug•L
mg/I. Acid I krbicidcs
ug.lL
ug/l. Semi,oln(iles
ugll, I Pll-l>icsel Range
ugil.
<0.2 UJ:lll. ' \"olatile Org~11ics t \"0.-\ boUlcJ
mg'L
mg'L I Pl l•(i;isoliuc Range
ug/1. I f'l{.l] I EX Gasoline Range
mg•L
ug•L
ugll.
ug•l.
U_l.''I.
1G0711 APR
-· ....
GROUNDWATER FIELD/LAB FORM
Counly I r:e 4'-. CI
Quad No L (, 7 1--Se,ial No. ______ _
Lal. 3)" 'i3 1 Q/11 1\I Long. /~LJG·.;·7',SY'1 t,)
Report To: ARO, FRO,(M~ RRO, Wano, WiRO,
SAMPLE PRIORITY
~llOUTfNE □EMERGENCY
-EZJcHAIN or CUSTODY
WSRO, l<inston FO, Fed. Trust, Cenlral 011., Oilier: ______ ~--
Shipped by: □us, ~;i, I land Del., Oilier·
r~ o r t h C a r o I i 11 a
Depatlment or Envlroruncnl, I lcallh, and Natu, al ncsourc:es
DIVISION OF ENVlnONMENTAL MANAGEMEIH -GllOUNDWATEll SECTION
0
Lab Number ~ D 1 IJ _
Date fleceild~~9::J __ Tiffle J~]._,l)~_
nec·u by: F,0111: Uus Cou<ier I land Del.,
Other: _________________ _
Data Entry By: ______ Ck: ______ _
Dale Repo,ted: _____________ _
-/--/----------Pwpose:
Collector(s): ))c\,.,le,c, Date 1/ 7,/i') Time /,! ."Jo Baseline, Co111plainl, Co111pliance,.LUST, Peslicide S!udy, Federal ·11usl, O11,er: / I I 1cnl& ooo)
FIELD ANALYSES { 7 ° Owner -~C~l~vqf..Ll·~i>=c~,~-'~s'~>" •~k~,_I~'-~"'~·~•'-'-'-=~'~'~--------· ------------
pH,oo -~.s-Spec. Cond.94 7/ al-25° C Localion or site _;S'-''"-''-""'-'·'-'l-,--..="-·\..,,=,.,1-"'--,----,-------,----,----,----c----------
Temp. 10 / 0c Odor Description of sa111pling point .s1a 15d /,.':3 ,9cd '--\, j ,-4-:s ,_;c, (. d;,-',-
1\ppearance C(qo ~cc.{,::.-Gv,-· Sampling Method ----,,-----,"='+·~=--------Sample Interval ________ _ :\e;/ ~.iiiler,&tc) / FieldllnalysisBy: j)c./,/i Remarks v:<~ ~,-,,,_1,0 ;vu <z,v<{
LABORATORY ANALYSES (pempiaghm•.••lomp . .,,) ./
BOD 310 mq/1 Diss. Solids 70300 mgtl Aq · Silver 4G566 ugil O,ganochlorirte Pesticides --COD High 340 mg/I Flouride 951 m~I Al -Aluminum 46557 ug/1 01ganophosphorus Pesticides
COD Low 33S mg/I Hardness: T olal 900 mg/I As • Arsenic 46551 · ug/1 Nilrogen Pesticides ----Coliform: MF Fecal 31616 11001111 Hardness (non-carb) 902 nigll Ba• Bmium 46558 ug/1 --
Colilorrn: MF Tolal 3 I 504 /I00rnl Phenols 32730 ug!L_ Ca• Calcium 46552 rnq/1 Acid 1-/erl.iicides
TOC 680 mgll_ __snecilic Cond. 95 uMhos/cm2 Cd • Cadmium 46559 ug/1 --Twbidily 76 NTU Sulfale 945 mgll Cr -Chromium 46560 ugll Se111ivolatile O,ganics
Residue., Suspended 530 1119/I Sullido 745 111gtl Cu -Coeeer 4GSG2 ug~
Fe -Iron 46563 ugll
~ Hg -Mercu•t 71900 ugll ~ Volalile Organics (VOA bollle)
pH 403 units K -Potassium 46555 mg/I
Alkalinily lo pH 4.5 410 mg/I Mg -Magnesium 46554 mg/I TPH -Gasoline Range --Alkalinily lo pH 8.3 415 mgll Mn• Manqanese 46565 uall TPH -Bl EX Gasoline nange
Carbonale 445 mg/I NH, as N 610 rnq/1 Na -Sodium 46556 mq(I --Bica, bona le 440 1119/I _Uili_asJ'l.Ji2, mgll_ --Ni -Nickel ugll --' --
Ca1bon dioxide 405 mg~ ¼ t:IQ,-±ll__Q, as N 630 11191_ Pb -Lead 46564 ugl) --i/
Chloride 940 111gll P: Tolal as P 665 mq/1 Se -Selenium uq/1 V --Cluomium: Hex 1032 ugll Zn -Zinc 46567 ugll --Color: Twe oo Pi-Co --Cyanide 720 mg/I
Lab Comments:---------------------------------------------------------
GW-54 REV. 6193 r-or Dissolved /\nc1.lysis -submit filtered sample and w,ite ''DIS'' in block.
EHNR/OWQ LABORATORY LAB NO. 7G0777
VOLATILE ANALYTICAL REPORT
REPORTED BY CG~ SUPEHVISOR ~'tt 1,#t{.{l__ CHECKED BY -¥ DATE
REVIEWED BY IJff!,,-
SAMPLE TYPE: WATER ANALYSIS RESULTS
75-35-4 1, 1-Dichloroethene 0.75 u 96-18-4 1,2,3-Trichloropropane 0.25 u
75-09-2 Methylene Chloride 10 u 108-86-1 Bromobenzene u
156-60-5 tr ;i11s-1,2-0ichloroe\11ene 0.75 u 95.49.5 2-Chlorotoluene 0.25 u
75-34-3 1, 1-Dichloroethane 0.25 u 106-43-4 4-Chlorotoluene 0.25 u
590-20-7 2, 2-Dichloropropane 0.25 u 541-73-1 1,3-Dichlorobenzene 0.25 u
156-59-4 cis-1,2-Dichloroethene 0.25 u 106-46-7 1,4-Dichlorobenzene 0.25 u
67-66-3 Chloroform 0.25 u 95-50-t 1,2-Dichlorobenzene 0.25 u
74-97-5 Bromochloromethane 0.75 u 96-12-8 1, 2-Dibromo-3-Ch1oropropane u
71-55-6 1. 1, 1-Trichloroethane 0.25 u 120-82-1 1,2,4-Trichlorobenzene 0.25 u
563-58-6 1. 1-Dichloropropene 0.25 u 87-68-3 Hexachlorobutadiene 0.25 u
56-23-5 J Carbon Tetrachloride 0.75 u 87-61-6 1,2,3-Trichlorobenzene 0.75 u
107-06-2 1,2-Dichloroethane 0.25 u 1634-04-4 Melhyl-tert-butyl ether 5 u
79-01-6 l richloroethene 0.25 u 71-43-2 Benzene u
78-87-5 1.2-Dichloropropane 0.25 u 108-88-3 Toluene u
75-27-4 Bromodichloromelhane 0.25 u 100-41-4 Ethyl benzene 1 u
74-95-3 Dibromomethane u 108-38-3 m,p-Xylenes 2 u
10061-01-5 cis-1,3-0ichloropropene 0.25 u 95-47-6 a-Xylene u
1006 t-02-6 tr a ns-1, 3-Did1loropropene 0.25 u 100-42-5 Styrene u
79-00-5 1.1.2-Trichloroethane 0.25 u 98-82-8 lsopropylbenzene u
127-18-4 Tetrachloroethene 0.25 u 103-65-1 n-Propy1benzene u
142-28-9 1.3-0ichloropropane 0.25 u 108-67-8 1.3,5-Trimethylbenzene u
124-48-1 Dibromochloromethane 0.75 u 98-06-6 lert-Butylbenzene u
106-93-4 1,7-Dibromoelhane 1 u 95·63-6 1.2,4-Trimethylbenzene u
108-90-7 Ct1lorobenzene 0.25 u 135-98-8 sec-Butylbenzene u
630-20-6 1.1. 1,2-Telrachloroe\hane 0.25 u 99-87-6 p-isopropyltoluene u
75-25-2 Bromoforrn 0.5 u 104-51-8 n-Butylbenzene u
79-34-5 , 1,2,2-Telrachloroethane 0.75 u 91-20-3 Naphthalene u
rngll mgtl
TQL-Target Quanlilation Limit-Subject lo Gasoline Range Estimated Total Petroleum Hydrocarbon 0.25 N
change due to instrument sensitivity
T-Ter1talively Identified, not confirmed Other purgeables detected Detected
E-Esfonaled Value (up to 10 highest peaks) ug/L
U-Samples analyzed ror this compound but not detected
N-Sample not analyzed for this compound NO VOlATILE ORGANIC COMPOUNDS
0-Detected below quantilation limit DETECTED BY GC/ELCD/PJD.
M-GCIMS Analysis performed
COMMENTS:
,..
COUNTY
QUAD NO:
IREDELL
RECEIYED/EHHR
lJ[r1. GHOIJHD W/1TEH SEC.
911\PR 24 Pi\ l: 20
~~~~:~;iR(S) : c~c'AcRlc~7L7EcNc-_______ Regional Office
DATE: 4n/'J1
TIME:
PURPOSE:
LABORATORY ANALYSIS
BOD JIO
COD High 340
COD LowJJS
Coliform: MFF=ilJ1616
Coliform: MFTotalJl504
TOC
Turbitity
Residue., Suspended 530
Total Suspended solids
pH
Alkn!inity lo pll 4.5
Alka!inily to pll 8.3
Caibonate
Bicaibonate
Carbon dio1tide
Chlo,ide
Chromium· Hex IOJ2
Color: True HO
Cy11nide 720
COMMENl'S:
mg/L
rng/L
rng/L
1100ml
1100ml
mg/I
NTU
rng/L
rng/L
units
m~L
mg/L
mg/L
mg.IL
rng/L
mg/L
ug/L
e.u.
mg,L
Owner:
Location or Site:
Description of s..,mpling point
Sampling Mcehod·
Remarh
Uiss. Solids 70300
Fluoride 95 I
I lardness: local 900
I lardnen: {non-c111b) 902
Phenols J27JO
Specific Cond. 95
Sulfate
Sulfide 745
MBAS
Oil and Grease
Silica
Uonm
l'ormaldehyJe
NIIJ as N 610
f'KN as N 625
N02 +NOJ as n 6JO
r: Total as P 665
ro,
lJl\'ISION OF \\'ATER QUALITY
Chtn1is1ry· L11bon1lory Rtpotl I Ground W111er Qu11til)
~_AMPLI; PRlQ_RIT\'.
(S]ROUl'INE
e] CIIAIN OF CUSTODY
EJ SAM PU; TYPE
DAVIDSON WELL Ill
rng/L
rng/L
mg/L
mg/L
ug/L
uMhos/cm2
rng/L
. rng/L
mglL
1ng/L
mg.IL
mg.IL
rng/L
mgJL
mg/L
mg/L
mgfL
□EMERGENCY
□
Ag-Silver 46566
Al-Aluminum 46557
As-Arsenic 46551
B:i-Bwium 46558
Ca-Calcium 46552
Cd-Cadium 46559
Cr-Chromium 46560
Cu-Copper 1042
Fe-Iron 1045
1 lg-Me,cury 71900
K-l'otassium 46555
~lg-~lagncsium 927
~111-~langanese 1055
Na· Sodium 929
Ni-Nicl..cl
rb-Lead 46564
Se-Selenium
'" Zmc 46567
-
Lab Number 7G0778
Date Re(:ei,ed 418197
Time Rccci\'ed 9.00AM
Recei,·ed lly DS
Rdeased lly us
Da1c "poned : 412J/97
ugiL Organochl01ine Pesticides
ug/L Organophosphorus Pesticides
ug1L NillO!;!en Pesticides
u!!fL
mgll ,\cid llerbicides
ui;/L
ug!L ' Scrni,olatiles
ug/L Tl'II-Uiescl Rnnge
ugiL
ug/L ' \"olatile Orga11ics t\'OA bouleJ
mg!L
111g1L I 1'11-Uasolinc llnngc
uglL I PII-UfEX Gasoline lla11ge
111g/L
ug,L
ug!L
ugll
ug'L
1G0718 APR
~
GROYNDWATER FIELD/LAB FORM
County -,P..c!.,__ l 1
Quad No l.(, 7,-,.,
Lal. _;p·• 1./J.' 5Y11N
Serial No. ______ _
Long. f:u-~-7' ~ ]' '' t J
Report To: /\RO, FA~ RRO, WaAO, WiRO,
SAMPLE PRIORITY
8:JnoUTINE □EMERGENCY g]c1 IAIN OF CUSTODY
WSRO, Kinston FO, Fed. Trust, Central Oil., Other: _________ _
Shipped by: Bus,<Courla\<, Hand Del., Other_· ___________ _
tJ o r l h C n r o I I II a
DCpatlmenl of Envlro111nc111, lfcallh, nnd Nalurnl RC?sources
DIVISION OF ENVIRONMENTAL MANIIGEMENr -GnOUNUWATER SECTIOH
Lab Number
0 Dale Receiv _ _ ':JSlJ._
llec"d by:_ From: Bus.er, I land Del.,.
Ol11er: ________________ _
Data Entry By: ______ Ck: ______ _
Dale Reported: ______________ _
"~ / Pu,pose:
Colleclor(s): Yeh I "-o · Dale • £/115? Time / J .' •'5 Baseline, Complain!, Compliance, LUST, Peslicido S!udy, Federal 1rusl, Other: G-v :r:: ... -;Ji ?~ J. L f-t _ 1c11cle ono) FIELD ANALYSES e Owner ,,__,_,<1$ (• , :li -. ' --7./ I pH400 ~J · '-"Spec. Cond.94 --'c,,~-al2&" C Location or site ---'--JL_----=------,--,----------------------
Ternp.10 /8 °c Odor Description ol sampling point ~-"-'-<:...,--'cL-"=•lesc,,,,_,:cs. ___________________ _
Appearance </«-, /,·~(~~l,__,f Sampling Method-~-------__________ Sample Interval _______ _ V 1/ { t~Jl. bai!or, otc I Field Analysis By: j),; ~¼--,,.< Remarks IC I-... C ..... ,~ ===-=.-----------------
fpvmpini;i limo, air l9mp. elc.) LABORATORY ANALYSES
BOD, 310 mg/I Diss. Solids 70300 mg{! Ag -Silver 46566 ugil O,ganochlorine Pesticides
COD High 340 mg/I .Flouride 951 1119/I Al -Aluminum 46557 ug!I --O1grinophosphorus Pesticides COD Low 33S n,gtl Hardness: Total 900 mg/I As -Arsenic 46551 uq/1 Nit,ogen Pesticides
Colilorm: MF Fecal 31616 /100ml Hardness (non-carb) 902 mgtl Ba -Barium 46558 uq/1 --· Colilorm: MF Tolal 31504 /I 00ml Phenols 32730 ug/1 Ca -Calcium 46552 mg/I Acid Herbicides
TOG 6B0 1I1Clil Specific Cond. 95 uMhos/cm2 Cd -Cadmium 46559 un1J --T urbidi!r 76 NTU Sulfale 945 rng!'.I Cr -Chromium 46560 UtJfl I>< Se111ivolatile O1ganics
Residue., Suspended 530 mg/I Sulfide 745 mg{I --Cu -Coeeer 46562 ug/1
Fe • Iron 46563 ugtl
Hg -Mercurr 71900 ugll >< Volalile Organics (VOA boll1e)
pH 403 unils K • Potassium 46555 mg/I
Alkali11ily lo pH 4.5 410 mg/I Mg -Magnesium 46554 mq{I TPH -Gasoline Range --Alkalinily lo pH 8.3 415 mg/I Mn -Manaanese 46565 uail ·r PH -B1 EX Gasoli11e Range
Carbonale 445 mg/I NH, as N 610 mg/I Na -Sodium 46556 mgtl
Bicarbonale 440 mnil JKtJ as tJ 625 mgLI Ni· Nickel ugil f7⇒2 Carbon dioxide 405 mg/I NO + NO as N 630 mgtl Pb -Lead 46564 ug/1 --Chloride 940 mg/I P: To!al as P 665 mg/I Se• Selenium ug/1
Chromium: Hex 1032 ug/1 Zn -Zinc 46567 ugll
Color: True ao Pt-Co --Cyanide 720 mg/I
Lab Comments:---------------------------------------,--------------------
GW-54 REV. 6'93 For Dissolved Analysis -submil fillered sample and write "DIS" in block.
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
62-63-3
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-6
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95.95.4
91-58-7
99.74.4
131-11-3
208-96-8
WATER
ANILINE 10
PHENOL 10
BIS(2-CHLOROETHYL) ETHER 10
2-CHLOROPHENOL 10
1,3-DICHLOAOBENZENE 10
1.4-DICHLOROBENZENE 10
BENZYL ALCOHOL 20
1,2-DICHLOROBENZENE 10
2-METHYL PHENOL 10
8IS(2-CHLOROISOPROPYU ETHER 10
4-METHYL PHENOL 10
N-NITROS0-01-N-PROPYLAMINE 10
HEXACHLOAOETHANE 10
NITRO BENZENE 10
ISOPHORONE 10
2-NITRO PHENOL 10
2,4-DIMETHYL PHENOL 10
BENZOIC ACID 50
BIS(2-CHLOAOETHOXY) METHANE 10
2,4-DICHLORO PHENOL 10
1,2.4-TRICHLOROBENZENE 10
NAPHTHALENE 10
4-CHLOROANILINE 20
HEXACHLOROBUTADIENE 10
4-CHLOA0-3-METHYL PHENOL 20
2-METHYL NAPHTHALENE 10
HEXACHLOROCYCLOPENT ADI ENE 10
2.4,6-TAlCHLOAO PHENOL 10
2,4,5-TRICHLORO PHENOL 10
2-CHLOAO NAPHTHALENE 10
2-NITROANILINE 50
DIMETHYL PHTHALATE 10
ACENAPHTHYLENE 10
EHNR/DWQ LABORATORY
SEMI-VOLATILE ANAL.YTICAL REPORT
ANALYSIS RESULTS
u 606-20-2
u 99-09-2
u 83-32-9
u 51-28-5
u 100-02-7
u 132-64-9
u 121-14-2
u 84-66-2
u 7005-72-3
u 86-73-7
u 100-01-6
u 534-52-1
u 86-30-6
u 101-55-3
u 116-74-1
u B7-B6-5
u B5-01-B
u 120-12-7
u 84-74-2
u 206-44-0
u 129-00-0
u 85-68-7
u 91-94-1
u 55.55.3
u 218-01-9
u 117-81-7
u 117-84-0
u 205-99-2
u 207-08-9
u 50-32-8
u 193-39-5
u 53-70-3
u 191-24-2
2,6-DINITROTOLUENE
3-NITROANIUNE
ACENAPHTHENE
2.4-0INITRO PHENOL
4-NITRO PHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANlLINE
4,6-DINITR0-2-METHYL PHENOL
N-NITAOSOOIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
I IEXACHLOROBENZENE
PENT ACHLOAO PHENOL
PHENANTHAENE
ANTHRACENE
DI-N-BUTYL PHTHALATE
FLUORANTHENE
PY RENE
BUTYLBENZYL PHTHALATE
3,3 .. ·DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHAYSENE
BISI2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYL PHTHALATE
BENZO(BJFLUORANTHENE
BENZO(K)FLUORANTHENE
BENZOIA)PYRENE
INDENOI 1,f,3-CDIPYRENE
DlBENZO(A,H)ANTHRACENE
BENZO(G,H,IJPEAYLENE
LAB NO. 7G0778
SUPERVISOR ·-r_f_ ./(
10
50
10
50
50
10
10
10
10
10
50
50
10
10
10
50
10
10
10
10
10
10
20
10
10
10
10
10
10
10
10
10
10
7
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
SEMIVOLATILE ORGANICS REPORT -DWQ LAB PAGE 2
NO BASE/NEUTRAL OR ACID EXTRACT ABLE ORGANICS
DETECTED BY GC/MS.
LAB NO. 7G077B -----
TOL-Target Ouantitation limit-Subject to
change due to instrument sensitivity
T-Tentatively Identified, estimated concentration
E-Estimated Value
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound
D-Detected below quantitation limit
H-Holding time exceeded
COMMENTS: ___________________________________________________ _
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
75-35-4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79-34-5
TQL-
T-
E-
U-
N-
0-
M-
COMMENTS:
WATER
1, 1-Dichloroelhene 0.75
Methylene Chloride 10
trans-1,2-Dichloroethene 0.75
1, 1-Dichloroethane 0.25
2,2-Dichloropropane 0.25
cis-1,2-Dichloroethene 0.25
Chloroform 0.25
Bromochloromethane 0.75
1, 1.1-Trichloroethane 0.25
1, 1-Dichloropropene 0.25
Carbon Tetrachloride 0.75
1,2-Dichloroethane 0.25
Ttlchloroethene 0.25
1.2-Dichloropropane 0.25
Bromodichloromethane 0,25
Dibromomelhane 1
cis-1,3-Dichloropropene 0.25
trans-1,3-Dichtoropropene 0.25
1, 1.2-Trichloroethane 0.25
Telrachloroethene 0.25
1,3-Dichloropropane 0.25
Dibromochloromelhane 0.75
1.2-Dibromoethane
Chlorobenzene 0.25
1. 1.1.2-Tetrachloroethane 0.25
Bromoform 0.5
1, 1,2,2-Tetrachloroethane 0.75
Target Quanlitalion Limit-Subject to
change due to instrument sensitivity
Tentatively Identified, not confirmed
Estimated Value
Samples analyzed for this compound but not detected
Sample not analyzed for this compound
Detected below quantilation limit
GC/MS Analysis performed
EHNR/DWQ LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 96-18-4 1,2,3-Trichloropropane
u 108-86-1 Bromobenzene u 95-49-8 2-Chlorotoluene
u 106-43-4 4-Chlorotoluene u 541-73-1 1, 3-Dichlorobeniene
u 106-46-7 1,4-Dichlorobenzene u 95-50-1 1.2-Dichlorobenzene u 96-12-8 1,2-Dibromo-3-Chloropropane u 120-82-1 1,2,4-Trichlorobenzene u 87-68-3 Hexachlorobuladiene
u 87-61-6 1,2,3-Trichlorobenzene u 1634-04-4 Melhy1-lert-butyl ether u 71-43-2 Benzene
u 108-88-3 Toluene
u 100-41-4 Elhyl benzene u 106-38-3 m,p-Xylenes
u 95-47-6 o-Xylene
u 100-42-5 Styrene
u 98-82-8 lsopropylbenzene
u 103-65-1 n-Propylbenzene
u 108-67-8 1,3,5-Trimelhylbenzene
u 98-06-6 tert-Bulylbenzene u 95-63-6 1,2,4-Trimelhylbenzene
u 135-96-6 sec-Butylbenzene
u 99-87-6 p-isopropyltoluene u 104-51-8 n-Bulylbenzene
u 91-20-3 Naphthalene
Gasoline Range Estimated Total Petroleum Hydrocarbon
Other purgeables detected
(up to 10 highest peaks)
NO VOLATILE ORGANIC COMPOUNDS
DETECTED BY GC/ELCD/PID.
LAB NO. 7G0778
SUPERVISOR~
DATE~
ENTERED B
DATE i ID
0.25 u
1 u
0.25 u
0.25 u
0.25 u
0.25 u
0.25 ti
1 u
0.25 u
0.25 u
0.75 u
5 u
u
u
1 u
2 u
u
u
u
u
u
u
u
u
u
u
u
mg/L _mg/L
0.25 N
Detected
ug/L
HECEIVED!,fHNR SEC. DEt',. GROUl\O 'i,1-•JER
91 f1PR 24 PM \: ZO
COUNTY !REDELL
QUAD NO:
REPORT TO J\IRO __________ Regional Office
COLLECTOR(S) DAIILEN
DATE· 411191
TIME:
PURPOSE:
LABORATORY ANALYSIS
BOD JIO
COD lligh 340
COD Low JJ5
Coliform: MFFecalJ16J6
Coliform: MFTotalJlS04
roe
Turbitity
Residue., Suspended SJ0
Total Suspended solids
pll .
Alkalinity lo pH 4.S
Alkalinity lo pH 8.J
Carbonate
Bicarbonate
Cmbon dioxide
Chloride
Chromium· llex 1032
Cnlor: True 80
C')·11nide 720
COMJ\IENTS:
mg/L
mgiL
mg/L
1100ml
1100ml
mg/I
NTU
mg/L
mg/L
units
mg/L
mg/L
mg/L
mg/L
mg/L
mg.1L
ug'L
c.u
mgiL
(h,ucr:
Loca1ion or Si1e·
tkseriplion of sampling poin1
Sampling Method:
Remarks:
Diss. Solids 70100
l'luo,ide 951
JiaJdness: total 900
Hardness· {non-ca1b) 902
Phenols 12730
Specific Cond. 95
Sulfate
Sulfide 745
MBAS
Oil and G1ease
Silica
Boron
Formaldehyde
NHJ as N 610
TKN as N 625
NO2 +NO) as n 630
r: Total as P 665
ro,
IJl\'ISION OF WATER QUALIT\'
Chemistry L11lionlory Rfrort / Grnund W111er Qu,dity
SAMPI E PRIQRITY
E)ROUTINE
[] CHAIN OF CUSTODY
Ej SAMPLE TYPE
('.llltlS IIA\'lllS()N HENTAI.
mg/L
ms'L
mg/L
mg/L
,g/L
uMhos/cm2
mg/L
mg/L
mg/L
mg/L
111sfL
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
□EMERGENCY
□
Ag-Sil-~ 46566
Al-Aluminum 46557
As-Arsenic 46551
Ba-Barium 46558
Ca-Calcium 46552
Cd-Cadium 46559
Cr-Chromium 46560
Cu-Copper 10.12
Fe-Iron 1045
I lg-Mc,cury 71900
K-ro1assium 46555
Mg-Magnesium 927
t,.\n-Mm1ganese 1055
Na-Sodium 929
Ni-Nickel
Pb-Lead 4656-1
Se-Selenium
Zn_Zinc -H,5(,7
Lab Numb<:r 7G0780
Oat,: RcceiHd ; 4/8/97
Time Recei,cd 900,\/1.1
Recci,cd Br DS
Re/cased Uy us
Oa1c 1cpo1ted · 4/2J/V7
ugil. O,ganochlo,inc resticides
Ug/1. Organophosphorus Peslicides
.
Ug/L Nitrogen Pcs1icides
uglL
mg.'L Acid lkrbicidcs
ug/L
ug!l. X Semi,olatilcs
ug.'L l'rl I-Diesel Range
ug/L
,g!L X \'ola1ilc Organics (VO,\ bottle)
mglL
mg!L rPII-Gasolinc Range
ug/l. l'PI 1-ll TEX tiasolinc Range
mgrL
ug•L
ug'I.
ug'L
ug•l.
7G0780APA
-GRQ.IJl'JDWATER FIELD/LAB FORM
Report To: ARO, FRO~ ARO, WaRO, WiRO,
SAMPLE PRIORITY
~llOUTINE □EMERGENCY
121CHAIN OF CUSTODY
WSRO, l<inslon FO, Fed. Trust, Central 011., OIiier: _________ _
Shipped by: Bus, e~ Hand Del., Other_·----------~-
Uorth Cntol/110
Ocpa1tmcml ol Envlro111nc111, llcallh, n11d Nalurnl ncsou1ccs
'DIVISION OF ENVIRONMENTAL MANAGEMENT -GROUIIDWATER SECTION
0
Lab Number ~ D
Date neceiv~d --~-_Tin0)tfil ·
Rec'd by: r,0111: Bus, ourier Hand Del.,
Other: _________________ _
Data Entry By: ______ Ck: ______ _
Dale Reported: ______________ _
,,,,., Purpose:
Colleclor(s): J>s h I e,,,.. Dale Y/7! i 7 Time ~/~J~--'_J_) __ --s:..Baseline, Complaint, Cornpli
FIELD ANAL'(aES 1 ce, _LUST. Pesticide Sludy, Federal Trusl, Ollrer: 6-w f'-,u Jg,;/"' J't L
1c11cl11 OO(I)
17
al-25" C
Owner_,,.=.a...1_..u.s.c,.=,.,,._'""'"-",1-'-."-"--'-'""-½'------------------------
Location or sile 173 l'.'.,; "'a:,.-, r i),, :.,.._ pH,00 .,,-J · @Spec. Cond.94 57
Temp.10 /7 °c Odor _____ _
Appearance r = / c.;,&-{_._a
Description or sampling point -~.,":,""='::,;,.,_,Jco.--'-'~· _.,51-'-'J'-'A----'"=-t!J_. _z;-=''-"""V--"----------------r .J V
Field Analysis By: __ _j~'-)_,.~l..._¾.-=~-------
LABORATORY ANALYSES
~::~~~i~; M;~;r rbn £-e ~ S::: • ,.Q.ba-., .• "'I ________ Sample lnlerval
J {pompirn~llm11,ak"lo;;:mpC""_:Co<o'-) _________________ _
BOD, 310 mg/I Diss. Solids 70300 mg/I Ag -Silver 46566 ugll O,ganochlorine Peslicides --COD High 340 mg/I Flouride 951 ma,I Al• Aluminum 46557 uqll Organophosphorus Pesticides
COD Low 335 mgll Hardness: T ala! 900 rng/I As -Arsenic 46551 Ug/I Nitrogen Peslicides
Colilorm: MF Fecal 31616 1100ml Hardness {non-carb) 902 mgtl Ba -Barium 46556 ugll
Coliform: MF Total 3 t 504 /10011rl Phenols 32730 ug/1 Ca -Calcium 46552 mq/1 Acid Herbicides
TOC 680 mg1~ Specilic Cond. 95 --uMhos/cm2 Cd -Cadmium 46559 ua/I
Turbidity 76 NTU Sullate 945 ma,I Cr -Chromium 46560 ua/I x Sernivolalile O,ganics
Residue., Suspended 530 mg/I Sullide 745 rng:'.'.'.I Cu -Coeeer 46562 ugll_
Fe -hon 46563 ug!l -----· -•----··
--I-lg -Mercury 71900 UM'' l2S Volalilo Oruanics (VOA lmlllc)
pH 403 units K -Potassium 46555 mgl_l
/\lkalinity to pH 4.5 410 rng/I Mn -Maqneslum 46554 rnq/1 TPH -Gasoline Range
Alkalinity lo pH 8.3 415 mgll Mn -Manganese 46565 ugll TPH • BTEX Gasoline nange
Carbonate 445 mg/I NH, as N 610 mg/I Na -Sodium 46556 m~l --Bicarbonate 440 mg/I --_llill...as N s2s mgLL Ni. Nickel ug/1
Carbon dioxide 405 mgll NO, + NO, as N 630 mg/I Pb -Lead 46564 ug/I t-l Chloride 940 mg/I P: Total as P 6G5 nm/I Se -Selenium ugll .?-.,
Chromium: Hex 1032 ugll Zn -Zinc 46567 UOII 'v \ ./
Color: True 80 Pt-Co I
Cyanide 720 mgll
Lab Cornrnenls: --------------------------------------.--------------------
GW-54 nEV. 6193 For Dissolved Analysis -submit lillered sample and write ~DIS" in block.
-
EHNRIDWQ LABORATORY LAB NO. 7G0780 ~ SEMI-VOLATILE ANALYTICAL REPORT
REPORTED BY
CHECKED BY
REVIEWED BY r'ffJ-
SAMPLE TYPE: WATER ANALYSIS RESULTS 7
62-53-3 ANILINE 10 u 606-20-2 2,6-DINITROTOLUENE 10 u
108-95-2 PHENOL 10 u 99-09-2 3-NITROANIUNE 50 u
111-44-4 BIS(2-CHLOROETHYL) ETHER 10 u 83-32-9 ACENAPHTHENE 10 u
95-57-8 2-CHLOROPHENOL 10 u 51-28-5 2.4-DINITRO PHENOL 50 u
541-73-1 1.3-DICHLOROBENZENE 10 u 100-02-7 4-NITAO PHENOL 50 u
106-46-7 1,4-DICHLOROBENZENE 10 u 132-64-9 DIBENZOFURAN 10 u
100-51-6 BENZYL ALCOHOL 20 u 121-14-2 2,4-0INITROTOLUENE 10 u
95-50-1 1,2-DICHLOROBENZENE 10 u 84-66-2 DIETHYL PH TH ALA TE 10 u
95-48-7 2-METHYL PHENOL 10 u 7005-72-3 4-CHLOROPHENYL PHENYL ETHER 10 u
108-60-1 BIS(2-CHLOROISOPAOPYLJ ETHER 10 u 86-73-7 FLUORENE 10 u
106-44.-5 4-METHYL PHENOL 10 u 100-01-6 4-NITROANIUNE 50 u
621-64-7 N-NITAOS0-0I-N-PROPYLAMINE 10 u 534-52-1 4,6-DINITA0-2-METHYL PHENOL 50 u
67-72-1 HEXACHLOROETHANE 10 u 86-30-6 N-NITROSODIPHENYLAMINE 10 u
98-95-3 NI fROBENZENE 10 u 101-55-3 4-BROMOPHENYL PHENYL ETHER 10 u
78-59-1 ISOPHORONE 10 u 118-74-1 HEXACHLOAOBENZENE 10 u
88-75-5 2-NITAO PHENOL 10 u 87-86-5 PENT ACHLORO PHENOL 50 u
105-67-9 2.4-DIMETHYL PHENOL 10 u 85-01-8 PHENANTHRENE 10 u
65-85-0 BENZOIC ACID 50 u 120-12-7 ANTHAACENE 10 u
111-91-1 815(2-CHLOAOETHOXY) METHANE 10 u 84-74-2 Dl-N-BUTYL PHTHALATE 10 u
120-83-2 2,4-0ICHLOAO PHENOL 10 u 206-44-0 FLUOAANTHENE 10 u
120-82-1 1,2.4-TRICHLOROBENZENE 10 u 129-00-0 PYAENE 10 u
91-20-3 NAPHTHALENE 10 u 85-68-7 B-UTYLBENZYL PHTHALATE 10 u
106-47-8 4-CHLOAOANJUNE 20 u 91-94-1 3,3'-DICHLOROBENZIDINE 20 u
87-68-3 HEXACHLOAOBUTADIENE 10 u 56-55-3 BENZOiA)ANTHRACENE 10 u
59-50-7 4-CHLOR0-3-METHYL PHENOL 20 u 218-01-9 CHRYSENE 10 u
91-57-6 2-METHYL NAPHTHALENE 10 u 117-81-7 BI5(2-ETHYLHEXYL) PHTHALATE 10 u
77-47-4 HEXACHLOROCYCLOPENT ADJ ENE 10 u 117-84-0 DI-N-OCTYL PHTHALA TE 10 u
88-06-2 2.4,6-TRlCHLORO PHENOL 10 u 205-99-2 BENZO(BIFLUORANTHENE 10 u
95-95-4 2,4,5-TRICHLORO PHENOL 10 u 207-08-9 BENZO(K)FLUORANTHENE 10 u
91-58-7 2-CHLORO NAPHTHALENE 10 u 50-32-8 BENZOIA)PYRENE 10 u
88-74-4 2-NITAOANIUNE 50 u 193-39-5 INDENOl 1.-f,3-CD)PYAENE 10 u
131-11-3 DIMETHYL PHTHALATE 10 u 53-70-3 DIBENZOIA,HJANTHRACENE 10 u
208-96-8 ACENAPHTHYLENE 10 u 191-24-2 BENZO(G.H,l)PERYLENE 10 u
SEMIVOLATILE ORGANICS REPORT -DWQ LAB PAGE 2
NO BASE/NEUTRAL OR ACID EXTRACT ABLE ORGANICS
DETECTED BY GC/MS.
LAB NO. 7G0780 ------
TOL-Target Ouantitation Limit-Subject to
change due to instrument sensitivity
T-Tentatively Identified, estimated concentration
E-Estimated Value
U-Samples analyzed for this compound but not detected
N· Sample not analyzed ror this compound
D· Detected below quantitation limit
H-Holding time exceeded
COMMENTS, _______________________________________________ _
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
75-35-4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79-34-5
TOL-
T-
E-
U-
N-
D-
M-
COMMENTS:
WATER
1, 1-Dichloroethene 0.75
Methylene Chloride 10
trans-1,2-Dichloroethene 0.75
1, 1-Dichloroethane 0.25
2,2-Dichloropropane 0.25
cis-1,2-Dichloroethene 0.25
Chloroform 0.25
Bromochlorome\hane 0.75
1, 1, 1-Trichloroethane 0.25
1, 1-Dichloropropene 0.25
Carbon Tetrachloride 0.75
1.2-Dichloroethane 0.25
Trichloroethene 0.25
1,2-Dichloropropane 0.25
Bromodichloromelhane 0.25
Dibromomethane
cis-1,3-0ichloropropene 0.25
trans-1, 3-Dichloropropene 0.25
1, 1,2-T richloroelhane 0.25
T elrachloroethene 0.25
1,3-Dichloropropane 0.25
Dibromochloromelhane 0.75
1,2-Dibromoelhane 1
Chlorobenzene 0.25
1, 1, 1,2-Tetrachloroethane 0.25
Bromoform 0.5
1, 1,2,2-T elrachloroethane 0.75
Target Quanhtation limit-Subject to
change due to instrument sensitivity
T entalively Identified, not confirmed
Estimated Value
Samples analyzed for this compound but not detected
Sample not analyzed for this compound
Detected below quanlitalion limit
GC/MS Analysis performed
EHNRIDWQ LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 96-18-4 1,2,3-Trichloropropane u 108-86-1 Bromobenzene
u 95-49-8 2-Chlorotoluene
u 106-43-4 4-Chlorotoluene u 541-73-1 1,3-0ichlorobenzene
u 106-46-7 1,4-Dichlorobenzene
u 95-50-1 1, 2-Dichlorobenzene
u 96-12-8 1,2-Dibromo-3-Chloropropane
u 120-82-1 1,2,4-Trichlorobenzene u 87-68-3 Hexachlorobutadiene u 87-61-6 1,2,3-Trichlorobenzene u 1634-04-4 Melhyl-tert-bulyl ether
u 71-43-2 Benzene u 108-88-3 Toluene u 100-41-4 Ethyl benzene
u 108-38-3 m,p-Xylenes u 95-47-6 a-Xylene
u 100-42-5 Styrene
u 98-82-8 lsopropylbenzene
u 103-65-1 n-Propylbenzene
u 108-67-8 1,3,5-T rimethylbenzene u 98-06-6 tert-Butylbenzene u 95-63-6 1,2,4-Trirnethylbenzene u 135-98-8 sec-Butytbenzene u 99-87-6 p-isopropyltoluene
u 104-51-8 n-Butylbenzene
u 91-20-3 Naphthalene
G8soline Rang8 Estimated Total Petroleum Hydrocarbon
Other purgeables detected
(up to 10 highest Peaks)
NO VOLATILE ORGANIC COMPOUNDS
DETECTED BY GC/ELCO/PID.
LAB NO. 7G0780
0.25 u
1 u
0.25 u
0.25 u
0.25 u
0.25 u
0.25 u
u
0.25 u
0.25 u
0. 75 u
5 u
u
u
1 u
2 u
u
u
u
u
u
u
u
u
u
u
u
mg/L mg/l
0.25 N
Detected
ug/L
COUNTY·
QUAD NO:
!REDELL
fiECC:/VED/f//,'IR
DfM. GP.GU/-'{) \\'11/lj src.
97 ~PR 211 PM f: 20
REPORT TO _,_I_R00 _________ Regional Omcc
COLLECTOR(S) : 0D~Acl~IL~E~NC,--------
DATE: 417/97
TIME:
PURPOSE:
LABORATORY ANALYSIS
B00310 mg/L
COD High 340 mg/L
COD LowJJS mg/L
Colifonn; MF F«al 31616 1100ml
Colifom,: MF Total 31504 1100ml
TOC mg/I
Tu1bi1i1y NlU
Residue., Suspended BO mg.IL
Total Suspcndcd solids mg/L
pll uni1s
Alkalinity to pH 4.5 mg.IL
Alkaliniiy to pH 8.3 mg/L
Carbonate mg/L
Bicaibonalc mg/L
CNbon dio>tidc mg/L
Chlo,idc mg/L
Chromium: He>t 1032 ug/L
Color: True 80 "
Cyanide 7ZO mg/L
C0/\11\IENl"S:
Owner:
Localion or Site:
Description of sampling poin1
Sampling Method
Rema,ks·
Diss_ Solids 70300
Fluoride 95 J
1/;udncss: lotal 900
I lardneu: (non-carb) 902
l'henols 32730
S1><"cific Cood. 95
Sulfate
Sulfide 745
MBr\S
Oil and Grease
Silirn
lforun
Formaldehyde
NIIJ as N 610
!'KN as N 625
N02 ~ NOJ os n 630
I': Total as P 665
ro•
DIVISION OF WATER QUALITY
ChemUlry L11bot11lory R .. po..-t / Grn,rnd Wnlrr Qu11lily
SAMPLE PRIORITY
BJROUTINE □EMERGENCY
~ CIIAIN OF CUSTODY
~ SAMPLE TYPE □
DAVIDSON ROOFING WELL 112
mg/L Ag-Siher 46566
mg/L Al-Aluminum 46557
mg/L As-Arsenic 46551
mg/L Ba-Barium 46558
ug/L Co-Calcium 46552
uMhos/c,112 Cd-Cndium 46559
mg.'L Ci-Chromium 46560
mg/L-Cu-Copper I 042
mg.IL Fe-Iron I 045
mg/L Ilg-Mercury 71900
mg/I. K-l'ul;nsium 46555
/Ilg-Magnesium 927
mg/L /lln-/llauganesc 1055
mg/L Na-Sodium 929
mg1L Ni-Nidcl
mg/L l'b-lcad 46564
mgll Sc-Selenium
mg/L Zn Zinc 46567
I.ab Number 7G0776
Date Rccci, cd -'18191
Tim.-R.-cei, cd 900AM
Rccci,cd B\" DS
RclC'ascd By DS
Dale rcpollt'd · ·11231'17
ug/L 01g:mochlorine Pesticides
,git. 01ganophosphorus Pesticides
ug/L Niuogcn Pesticides
,~L
mg/1. ,\cid lkcbicidcs
ugil.
ug/l ' Scmi,ulatiles
ug1L Tl'II-Dicscl Range
ugll.
uglL ' Volatile O,ganics j\"QA bonlc)
m,.:11.
mg1L J'l'II-Uasoline Range
ug/L rrH-BH!X Gasoline Range
rng1l
,g1L
U!_:IL
ug/L
ug1L
1G0H6APR
GROUNDWATER FIELD/LAB FORM
Cciunly 'T;c-2 .j, ,y
Quad No (. b J '= /
Lal. 3I'S,21 5-'i '' N
Serial No.----,-----
P, p .---,/ -,;,I/, 1 Lonuu -' I \ T ~
Reporl To: ARO, FRO,<@, RRO, WaRO, WiRO,
SAMPLE PRIORITY
[BROUTINE □EMERGENCY
~CI-I/\IN OF CUSTODY
WSRO, Kinston FO, Fed. Trust, Central 011., Other: _________ _
I-I o r I h C a r o I i n a
0cpmlrmml of Environment, llcallh, nnd Natural ncsources
. , DIV,ISION OF ENVIRONMEIHAL MANIIGEMElff -GROUNDWATER SECTION
0
lab Number _:_li~~~ \e
Dale Received ~-fJJ..-Time 9.:trzi'----
nec'd by: D F,0111: Bus~ I land Del.,
Other: _________________ _
Data Entry By: ______ Ck: ______ _
Dale Reported: ______________ _
Shipped by: Bus~u r, Hand Del., Other· '-, I , ~ --Purpose:
Colleclor(s): lb Date L./CJ,/ f 7 Time 11 · j j Baseline, Complain!, CornplianceJLIJST, Peslicide Sludy, Federal Trusl, Olher: G:w .I:.,, +-i ;\,. . c11cle or>eJ FIELD ANALYSES :'.-6 owner v e;,usl,;,,,, ti.rtt J' _j LJ; It 2-.
pl·l,00 A-~-: 0 Spec. Cond.94 -~Z~/~_ a~° C Location or sile --------~--,-----,-----,--------------------
-ft.-D'.2 z..
Temp.10 iL 0c Odor_______ Description ol sampling poinl -~~,,f't2~,u771· ~,,__· ~,.•~•~·1~·7fr-~•-,Jl"-~{,,=,<~I,_, -----------------
Appearance ';. 1, r ,/ C?(,:,,l-~Y Sampling Melhod -------~,?:::,,~4.c==~-------Sample Interval ________ _ _ i<f§ipi bailG1, elc)
Field Analysis By: _____________ Remarks--'-'"'"'--'---'=~-"'->--"'=~---;;;;====="'----------------LABORATORY ANALYSES (p,mp,,gum,,, ... mp.o<c.)
BOD, 310 mg/I Diss. Solids 70300 mg/I Ao -Silver 46566 uq/1 Organochlorine Pesticides
COD High 340 mg/I Flouride 951 mg/I Al -Aluminum 46557 uq/1 Organopl1osphorus Pesticides
COD Low335 mg/I Hardness; Total 900 mg/I As -Arsenic 46551 Uq/l Nihogen Pesticides
Coliform: MF Fecal 31616 /1 OOrnl Hardness (non-carb} 902 mg/I Ba -Barium 46558 uq/1
Colilorm: MF Tolal 31504 /100ml Phenols 32730 ug/1 Ca -Calcium 46552 nm{I --Acid He1bicides --· TOC 680 mg/I Sgecilic Cond. 95 uMl1os/cm2• Cd -Cadmium 46559 un/J
Turbidill 76 NTU Sullale 945 m~I Cr -Chromium 46560 ug/1 ~ Se111ivolalile O,ganics
Residue., Suspended 530 mg/I Sullide 745 mg/I Cu -Coeeer 46562 ug/1
Fe • hon 46563 ug/1
Hg• Mercur~ 71900 ug/1 LX, Volalile Organics (VOA bottle)
pH 403 units K -Potassium 46555 mg/I
Alkalinily lo pH 4.5 4/0 rng/1 Mg -Magnesium 46554 mgJI TPH • Gasoline Range --Alkalinity lo pH 8.3 415 mg/I Mn -Manganese 46565 ug/1 TPH -BTEX Gasoline Range
Carbonate 445 mg/I NH. as N 610 mail Na -Sodium 46556 n,q/1
Bicarbonate 440 mg/I --_IBf.1 as f.1 625
--
rngll Ni· Nickel Ug/1
Carbon dioxide 405 mg/I NO + NO as N 630 mg/I Pb -lead 46564 Ua/1 , I
Chlorida 940 mg/I P: Total as P 665 mg/I Se -Selenium ug/1 V
Chromium: Hex 1032 ug/1 Zn -Zinc 46567 ug/1 --Color: True BO Pl-Co
Cyanide 720 mg/I
Lab Comments:---------------------------------------,-------------------
GW-54 llEV. 6193 · For Dissolved Analysis -submit fillered sample and write "DIS" in block.
~ EHNR/DWQ LABORATORY LAB NO. 7G0776
SEMI-VOLATILE ANALYTICAL REPORT
REPORTED BY -~ SUPERVISOR .. __ •
CHECKED BY ,a--;:; DATE / 7 -
REVIEWED BY ;'?/iJ
ENTERED B~ SAMPLE TYPE: WATER ANALYSIS RES UL TS DATE . ,., 1
62-53-3 ANILINE 10 u 6D6-20-2 2,6·DINITAOTOLVENE 10 u
108-95-2 PHENOL 10 u 99-09-2 3-NITROANIUNE 50 u
111-44-4 B1S12-CHLOROETHYLJ ETHER 10 u 83-32-9 ACENAPHTHENE 10 u
95-57-8 2-CHLOROPHENOL 10 u 51-28-5 2,4-DINITRO PHENOL 50 u
541-73-1 1,3-0ICHLOAOBENZENE 10 u 100-02-7 4-NITAO PHENOL 50 u
106-46-7 1.4-DlCHLOROBENZENE 10 u 132-64-9 DIBENZOFUAAN 10 u
100-51-6 BENZYL ALCOHOL 20 u 121-14-2 2,4-DINITROTOLUENE 10 u
95-50-1 1.2-DICHLOROBENZENE 10 u 84-66-2 DIETHYL PHTHALATE 10 u
96-48-7 2-MEl IIYL PHENOL 10 u 7005-72-3 4-CHLOROPHENYL PHENYL ETHER 10 u
108-60-1 BIS(2-CHLOROISOPROPYLI ETHER 10 u 86-73-7 FLUORENE 10 u
106-44-5 4-METHYL PHENOL 10 u 100-01-6 4-NITAOANILINE 50 u
621-64-7 N-NITROSO-DI-N-PROPYLAMINE 10 u 534-52-1 4,6-D1NITA0-2-METHYL PHENOL 50 u
67-72-1 HEXACHLOAOETHANE 10 u 86-30-6 N-NITROSODIPHENYLAMINE 10 u
98-95-3 NITAOBENZENE 10 u 101-55-3 4-BROMOPHENYL PHENYL ETHER 10 u
78-69-1 ISOPHORONE 10 u 118-74-1 HEXACHLOA08ENZENE 10 u
88-75-5 2-NITAO PHENOL 10 u 87-86-5 PENTACHLOAO PHENOL 50 u
105-67-9 2.4-DIMETHYL PHENOL 10 u 85-01-8 PHENANTHRENE 10 u
65-85-0 BENZOIC ACID 50 u 120-12-7 ANTHAACENE 10 u
111-91-1 BI5(2-CHLOROETHOXY) METHANE 10 u 84-74-2 D1-N-BUTYL PH TH ALA TE 10 u
120-83-2 2.4-DICHLORO PHENOL 10 u 206-44-0 FLUORANTHENE 10 u
120-82-1 1,2,4-TRICHLOAOBENZENE 10 u 129-00-0 PYAENE 10 u
91-20-3 NAPHTHALENE 10 u 85-68-7 BUTYLBENZYL PHTHALATE 10 u
106-47-8 4-CHLOROANILINE 20 u 91-94-1 3, 3' -DICHLOAOBENZlDINE 20 u
87-68-3 HEXACHLOAOBUT ADIENE 10 u 56-55-3 BENZO{AJANTHRACENE 10 u
59-50-7 4-CHLOA0-3-METHYL PHENOL 20 u 218-01-9 CHRYSENE 10 u
91-57-6 2-METHYL NAPHTHALENE 10 u 117-81-7 BISI2-ETHYLHEXYL) PHTHALATE 10 u
77-47-4 H EXACHLOAOCYCLOPENT ADIENE 10 u 117-84-0 DI-N-OCTYL PH TH ALA TE 10 u
88-06-2 2,4,6-TRICHLORO PHENOL 10 u 205-99-2 BENZO(B)FLUOAANTHENE 10 u
95-95-4 2.4.5-TRICHLORO PHENOL 10 u 207-08-9 BENZO(KJFLUORANTHENE 10 u
91-58-7 2-CHLOAO NAPHTHALENE 10 u 50-32-8 BENZOIAJPYRENE 10 u
88-74-4 2-NITROANILINE 50 u 193-39-5 INDENO(l ,,!,3-CD)PYRENE 10 u
131-11-3 DIMETHYL PHTHALATE 10 u 53-70-3 DIBENZO(A,HIANTHRACENE 10 u
208-96-8 ACENAPHTHYLENE 10 u 191-24-2 BENZO(G,H,IJPERYLENE 10 u
SEMIVOLATILE ORGANICS REPORT -DWQ LAB PAGE 2
NO BASE/NEUTRAL OR ACID EXTRACT ABLE ORGANICS
DETECTED BY GC/MS.
LAB NO.
TOL-Target Ouantitation Limit• Subject to
change due to instrument sensitivity
T-Tentatively Identified, estimated concentration
E· E'.Stimated Value
7G0776
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound
D-Detected below quantitation limit
H-Holding time exceeded
COMMENTS: _______________________________________________ _
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
75-35-4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79-34-5
TOL-
T-
E-
U-
N-
0-
M-
COMMENTS:
WATER
1, 1-0ichloroelhene 0.75
Methylene Chloride 10
trans-1.2-Dichloroethene 0.75
1, 1-Dichloroethane 0.25
2,2-0ichloropropane 0.25
ds-1.2-Dichloroethene 0.25
Chloroform 0.25
Bromochloromethane 0.75
1, 1, I-Trichloroethane 0.25
1. 1-Dichtoropropene 0.25
Carbon T elrachloride 0.75
1.2-Dichloroethane 0.25
Trichloroelhene 0.25
1.2-Dichloropropane 0.25
Bromodichloromethane 0.25
Dibromomelhane 1
cis-1.3-Dichloropropene 0.25
lrans-1, 3-Dichloropropene 0.25
1.1.2-Trichloroethane 0.25
Tetrachloroethene 0.25
1.3-Dichloropropane 0.25
Oibromochloromethane 0.75
1,2-Dibromoethane
Chlorobenzene 0.25
1, 1, 1,2· T etrachloroethane 0.25
Bromoform 0.5
1, 1,2,2-Tetrachloroethane 0.75
Target Ouantitation limit-Subject lo
change due to instrument sensitivity
Tentatively Identified, not confirmed
Estimated Value
Samples analyzed for this compound but not detected
Sample not analyzed for this compound
Detected below quantitalion limit
GCfMS Analysis performed
EHNR/OWQ LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 96-18-4 1,2,3-T richloropropane
u 108-86-1 Bromobenzene
u 95-49-8 2-Chlorololuene
u 106-43-4 4-Chlorotoluene
u 541-73-1 1,3-Dichlorobenzene
u 106-46-7 1,~-Dichlorobenzene
u 95-50-1 1.2-Dichlorobenzene
u 96-12-8 1,2-Dibromo-3-Chloropropane
u 120-82-1 1.2,4-Trichtorobenzene
u 87-68-3 Hexachlorobutadiene
u 87-61-6 1,2.3-Trichlorobenzene
u 1634-04-4 Methyl-tert-butyl et_her u 71-43-2 Benzene
u 108-88-3 Toluene
u 100-41-4 Ethyl benzene
u 108-38-3 m,p-Xylenes
u 95-47-6 a-Xylene
u 100-42-5 Styrene
u 98-82-8 lsopropylbenzene
u 103-65-1 n-Propylbenzene
u 108-67-8 1.3, 5-Trimelhylbenzene
u 98-06-6 tert-Butylbenzene
u 95-63-6 1,2.4-Trirnethylbenzene
u 135-98-8 sec-Butyl benzene
u 99-87-6 p-isopropylloluene u 104-51-8 n-Bulylbenzene
u 91-20-3 Naphthalene
Gasoline Range Estimated Total Petroleum Hydrocarbon
Other purgeables detected
(up to 10 highest peaks)
NO VOLATILE ORGANIC COMPOUNDS
DETECTED BY GCfELCD/PID.
LAB NO. 7G0776
0.25 u
u
0.25 u
0.25 u
0.25 u
0.25 u
0.25 u
1 u
0.25 u
0.25 u
0.75 u
5 u
u
u
1 u
2 u
u
u
u
u
u
u
u
u
u
u
u
mg/L mg!L
0.25 N
Detected
ugfL
COUNTY IREDELL
QUAD NO:
RECEIVED/EHNR
DEM. GROIJtlO W/\JER SE(;
91 APR 2li PM I: 20 DIVISION OF WATEU. Ql)AIJT\'
Cliuni~lry l.11l10n1lor,· Rr.,orl I Ground \\'11\fr Qunlity
SAMPLE PRIORITY
~ROUTINE □EMERGENCY
REPORT TO MRO
COLLECTOR(SJ DAHLEN
,,,.=,--------Regional Office ~ CHAIN OF CUSTODY □ DATE: 1,n,91
TIME:
PURPOSE:
LABORATORY ANALYSIS
BOD 310 mg/L
COD HighJ40 mg/L
COD Low J3S mg/L
Coliform: MF Fecal 31616 1100ml
Coliform: MF Total J 1504 1100ml
roe mg,1
Turbitity NTU
Residue., Suspended 530 mg/L
Total Suspended solids mg/L
pl! units
Alkalinity lo pll 4 S mglL
Alkalinity to pl! 8 J mg/L
Carbonate mgll
Bi~aibonale mg/L
Caibon dio>1ide mg/L
Chloride me'L
Chromium· llcll 1032 ug/L
Color: True 80 '" C)·anide 720 mg.IL
COMMENTS:
o .... ner·
Location or Site;
Dcscripcion of sampling poinl
Sampling Method:
Remarks·
Diss. Solids 70300
Fluoride 9S 1
Hardness: total 900
Hardness· (non-carb) 902
Phenols 32730
Specific Cond. 95
Sulfate
Sulfide 745
MBAS
Oil and Grea~
Silica
Uornn
Formaldehyde
NIU as N 610
"JKNasN625
N02 1 NOJ as n 630
I': To1al as P 665
1'04
~ SAMPLETYPE
ELMORE WELL
mg/L Ag-Sih·cr 46566
me'L Al-Aluminum 46557
mg/L As-Arsenic 46551
mg/L Oa-Oariu111 46558
•g/L Ca-Calcium 46552
uMhos/cm2 Cd-Cadium 46559
mg/L Cr-Chrnmium 46560
mg/L Cu-Copper I0-12
mg/L Fe-Iron 1045
mgtl Ilg-Me1cury 71900
mg/I. K-l'otassiuu, 4lo5S5
'-1g-Magnesiu,n '(!7
mg/L Mn-'-1an!!ru•e~ 1055
mg/L Na-Sodiu111 929
mWL Ni-Nid.d
mJ!}L Pb-Lead 4656-1
mglL Sc-Selenium
mg/L Zn_Zinc465{,7
I.ab Numher 7(;0779
Dale Recei, ed 4/8/97
Time Recri,ed q-oo ,\M
ReceiH,d By OS
Relca~d Br DS
Uate reported : 412)/97
ug..'L Organochlorine Pesticides
ug.lL 01ganophosphorus Pesticides
uglL Ni1rogen Pesticides
uglL
rngll ,\cid lle,bicidcs
uglL
ug!L X Semi,olatiks
us'L TPH-IJicscl Range
ug/L
U!!:iL X \"olatile O,ganics ! \"OA boule)
mgil.
mg,L 11'1 I-Gasoline Range
ug,L 11'11-D l'EX Gasoline Raugc
mg•I,
ug•I.
Ug.'L
ug•I.
ug1L
7G0119Af'R
North Carol/110
Dcpmtrncnl ol Envlror11ne111, llcallh, ond Nalwol ncsources ·GnOUNDWATER FIELD/LAB FOAM .. , ·, ,_,-DIVISION OF ENVIRONMENT/IL MANAGEMENT -GROUNDWATER SECTIOfJ
Counly z-~,.-J... Lt
Quad No Lie. 7 "b
Lat. ss·~ 'fJ-' ::,'{'' N
Serial No. ______ _
Long. eo" :, c!, U( 'I(..)
Report To: ARO, FRO,@RRO, WaRO, WiRO,
SAMPLE PRIORITY
~llOUTINE □EMERGENCY
0CHAIN OF CUSTODY
WSRO, f<inslon FO, Fed. Trusl, Central 011., OIiier: ________ _
Shipped by: Bus, ~r, Hand Del., Olher_· --,-----------
0 OIiier: _________________ _
Data Entry By: ______ Ck: ______ _
Dale Reporleu: ______________ _
Colleclor(s): U, I, ( ~ Date Y / 7 /q--z
FIELD ANALYSES r I
Purpose:_,.....---•---..,
Time -~/-3~.-~'-e~ __ Baseli11e· Complain('r.ornpliance, .LUST, Peslicido Study, r-ederal Trust, Otl,er:~~ ~ -1c11cl11 one) j) -.
pH,00 · --,1-:' IIJ Spec. Cond.94 </ u ~ C
Ternp.10 / f 0 c Odor 11.,,.__,_
Owner £( tnGr:~ We.,L I I 4'.,1, < Jc' ,,j '""·
Location or sile 13 2 Lc.,.ce.... '/)., ·({c::lu,,1/(, <&0,;7]
Description of sarn;ling poinl _ -r;a~'.71-<:,,...-~l ~c~;-~6~•~c~lc·~,a=•~~~,~L _________________ _
Appearance c-( a..4:-: / c·, {c,v6=C
Field Analysis By: 'j) c l,_L,__, ,
LABORATORY ANALYSES
BOD 310 mg/I
COD High 340 mgll
COD Low 335 mfl! --
Coliform: MF Fecal 31616 /100ml
Colilorm: MF Tolal 31504 1100ml
TOC sao mq!!
Turbidity 76 NTU
Residue., Suspended 530 111911
pH 403 units
Alkalini<y lo pH 4.5 410 mg/I
Alkalini<y to pl-I 8.3 415 mgtl
Carbonate 445 mg/I
Bicarbonate 440 mg/I --
Cai ban dioxide 405 mg!I --Chloride 940 mg/I
Chromium: Hex 1032 U~/I
Color: True so P<-Co
Cyanide 720 mgll
Sampling Melhod -------.--:;;--c?c, ·==-------Sample lnlerval _______ _ ~baH11r,olc}
Remarks--------------;:===-===.------------------trurnp1ng time, air lomp. etc.)
Diss. Solids 70300 mg/I Ag -Silver 46566 uqll O1ganocl1lmine Pesticides
Flouride 951 mqll Al -Aluminum 46557 ugll Organophosphorus Peslicides
Hardness: Total 900 mq/1 As -Arsenic 46551 ug/1 Nitrogen Pesticides
Hardness {non-carbl 902 mg/I Ba -Barium 46558 uall
Phenols 32730 ug/1 Ca -Calcium 46552 rn9!:I Acid He1bicides
SQecific Cond. 95 uMhos/cm2 Cd -Cadmium 46559 uall
Sulla<e 945 mqll Cr -Chromium 46560 ugll 12:<: Semivolatile Organics . --Sulfide 745 ma/I Cu -Coeeer 46562 ug_!I_
Fe -hon 46563 ug/I
Hg -Mercury 71900 ugll ->-< Volalile 01ganics (VO/\ bollle)
K -Potassium 46555 rng/l
. Ma -Maqnesium 46554 mall TPH -Gasoline Range
Mn -Manqanese 46565 ugll TPH · Bl EX Gasoline nange
NH, as N 610 111911 Na -Sodium 46556 rng/1
JKf1..as..l'L625 mg!J. Ni -Nickel ugll
N02 + N03 as N 630 nm/I Pb -Lead 46564 ugll I 7 ""1 1Z P: To<al as P 66S mg/I Se -Selenium ugll 'i I • C Zn -Zinc 46567 uqll
-
Lab Cornrnenls: -----------------------------~--------.--------------------
GW-54 REV. 6193 For Dissolved Analysis -submit filtered sample and write "DIS" in block.
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95.95.4
91-58-7
88-74-4
131-11-3
208-96-8
WATER
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1.4-DICHLOROBENZENE
BENZYL ALCOHOL
1,2-DICHLOROBENZENE
2-METHYL PHENOL
8I5(2-CHLOROISOPROPYL) ETHER
4-METHYL PHENOL
N-NITROSO-DI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITRO PHENOL
2,4-DIMETHYL PHENOL
BENZOIC ACID
8ISl2-CHLOROETHOXYl METHANE
2.4-DICHLORO PHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOAOANILINE
HEXACHLOROBUT ADIENE
4-CHLOR0-3-METHYL PHENOL
2-METHYL NAPHTHALENE
HEXACHLOAOCYCLOPENT ADIENE
2.4,6-TRICHLORO PHENOL
2,4,5-TRICHLORO PHENOL
2-CHLORO NAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
10
10
10
10
10
20
10
10
10
10
10
10
10
10
10
10
50
10
10
10
10
20
10
20
10
10
10
10
10
50
10
10
EHNR/DWQ LABORATORY
SEMI-VOLATILE ANAL.YTICAL REPORT
ANALYSIS RESULTS
u 606-20-2
u 99-09-2
u 83-32-9
u 51-28-5
u 100-02-7
u 132-64-9
u 121-14-2
u 84-66-2
u 7005-72-3
u 86-73-7
u 100-01-6
u 534-52-1
u 86-30-6
u 101-55-3
u 118-74-1
u 87-86-5
u 85-01-8
u 120-12-7
u 84-74-2
u 206-44-0
u 129-00-0
u 85-68-7
u 91-94-1
u 56-55-3
u 218-01-9
u 117-81-7
u 117-84-0
u 205-99-2
u 207-08-9
u 50-32-8
u 193-39-5
u 53-70-3
u 191-24-2
LAB NO. 7G0779
2,6-DlNITROTOLUENE 10 u
3-NITROANIUNE 50 u
ACENAPHTHENE 10 u
2,4-DINITRO PHENOL 50 u
4-NITRO PHENOL 50 u
DIBENZOFURAN 10 u
2,4-DINITAOTOLUENE 10 u
DIETHYL PHTHALATE 10 u
4-CHLOAOPHENYL PHENYL ETHER 10 u
FLUORENE 10 u
4-NITROANIUNE 50 u
4,6-DINITA0-2-METHYL PHENOL 50 u
N-NITROSODIPHENYLAMINE 10 u
4-BROMOPHENYL PHENYL ETHER 10 u
HEXACHLOROBENZENE 10 u
PENT ACHLORO PHENOL 50 u
PHENANTHRENE 10 u
ANTHAACENE 10 u
0I-N-BUTYL PHTHALATE 10 u
FLUORANTHENE 10 u
PYRENE 10 u
BUTYLBENZYL PHTHALATE 10 u
3,3'-DICHLOAOBENZIDINE 20 u
BENZO(A)ANTHRACENE 10 u
CHRYSENE 10 u
BI5(2-ETHYLHEXYU PHTHALATE 10 u
DI-N-OCTYL PHTHALATE 10 u
BENZO(BJFLUORANTHENE 10 u
BENZO(KJFLUORANTHENE 10 u
BENZO{A)PYRENE 10 u
IND ENO( 112,3-CD)PYRENE 10 u
DIBENZO(A,H)ANTHRACENE 10 u
BENZO(G,H.IJPERYLENE 10 u
SEMIVOLATILE ORGANICS REPORT -DWQ LAB PAGE 2
NO BASE/NEUTRAL OR ACID EXTRACT ABLE ORGANICS
DETECTED BY GC/MS.
LAB NO. 7G0779 -----
TOL-Target Ouantitation Limit• Subject to
change due to instrument sensitivity
T-Tentatively Identified, estimated concentration
E-Estimated Value
U-Samples analyzed for this compound but not detected
N-Sample not analyzed ror this compound
D-Detected below quanlitation limit
H-Holding time exceeded
COMMENTS, _______________________________________________ _
' EHNR/DWQ LABORATORY LAB NO. 7G0779
½ VOLATILE ANALYTICAL REPORT
REPORTED BY SUPERVISOR
CHECKED BY
REVIEWED BY ~
ENfERED BY
SAMPLE TYPE: WAlER ANALYSIS RES UL TS
75-35-4 1, 1-Dichloroelhene 0.75 u 96-18-4 1, 2,3-Trichloropropane 0.25 u 75-09-2 Methylene Chloride 10 u 108-86-1 Bromobenzene u 156-60-5 trans-1,2-0ichloroelhene 0.75 u 95-49-8 2-Chloroto!uene 0.25 u 75-34-3 1, 1-Dichloroelhane 0.25 u 106-43-4 4-Chlorololuene 0 25 u
590-20-7 2,2-Dichloropropane 0.25 u 541-73-1 1,3-Dichlorobenzene 0.25 u 156-59-4 cis-1,2-Dichloroethene 0.25 u 106-46-7 _ 1,4-Dichlorobenzene 0.25 u 67-66-3 Chloroform 0.25 u 95-50-1 1,2-Dichloro~enzene 0.25 u
74-97-5 Bromochloromelhane 0.75 u 96-12-8 1, 2-Dibromo-3-Chloropropane 1 u 71-55-6 1, 1, 1-Trichloroethane 0.25 u 120-82-1 1, 2,4-Trichlorobenzene 0.25 u 563-58-6 1, 1-0ichloropropene 0.25 u 87-68-3 Hexachlorobuladiene 0.25 u
56-23-5 Carbon T elrachloride 0.75 u 87-61-6 1,2,3-Trichlorobenzene 0.75 u 107-06-2 1,2-Dicllloroethane 0.25 u 1634-04-4 Methy1-tert-butyl ether 5 u
79-01-6 T richloroelhene 0.25 u 71-43-2 Benzene u
78-87-5 1,2-Dichloropropane 0.25 u 108-88-3 Toluene u
75-27-4 Bromodichloromethane 0.25 u 100-41-4 Ethyl benzene 1 u
74-95-3 Dibromomethane u 108-38-3 m,p-Xylenes 2 u
10061-01-5 cis-1,3-Dichloropropene 0.25 u 95-47-6 o-Xylene u
10061-02-6 trans-1,3-Dichloropropene 0.25 u 100-42-5 Styrene u
79-00-5 1, 1,2-Trichloroethane 0.25 u 98-82-8 lsopropylbenzene u
127-18-4 T etrachloroelhene 0.25 u 103-65-1 n-Propylbenzene u 142-28-9 1. 3-Dichloropropane 0.25 u 108-67-8 1,3,5-Trimethylbenzene u
124-48-1 Dibromochloromethane 0.75 u 98-06-6 tert-Butylbenzene u
106-93-4 1,2-Dibromoethane 1 u 95-63-6 1,2,4-Trimethylbenzene u
108-90-7 Chlorobenzene 0.25 u 135-98-8 sec-Bulylbenzene u
630-20-6 1, 1, 1,2-Tetrachloroethane 0.25 u 99-87-6 p-isopropylloluene u
75-25-2 Bromoform 0.5 u 104-51-8 n-Butylbenzene u
79-34-5 1, 1,2,2-Telrachloroethane 0.75 u 91-20-3 Naphthalene u
mg!l mgfl
TOL-Target Ouantilalion limit-Subject to Gasoline Range Estimated Total Petroleum Hydrocarbon 0.25 N
change due lo instrument sensitivity
T-Tentatively Identified, not confirmed Other purgeables detected Detected
E-Estimated Value (up lo 10 highest peaks) ug!l
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound NO VOLATILE ORGANIC COMPOUNDS
D· Detected below quanlilation limit DETECTED BY GC/ELCD/PID.
M-GC/MS Analysis performed
COMMENTS:
State of North Carolina
Department of Environment,
Health and Natural Resources
Mooresville Regional Office
James B. Hunt, Jr,, Governor
Jonathan B. Howes, Secretary
DIVISION OF WATER QUALITY
November 5,
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
A.A.A, Enterprises, Incorporated
1268 Eufola Road
Statesville, North Carolina 28677
Attention: Barry Sigmon
1996
RE: Notice of Violation
15A NCAC 2L Classifications and
Water Quality Standards Applicable
to the Groundwaters
Dear Mr. Sigmon:
Sigmon Septic Tank Service
Groundwater Incident #3422
Priority Rank: 205A
Class: AB
Iredell County, N,C,
Chapter 143, North Carolina General Statutes, authorizes and
directs the Environmental Management Commission of the Department
of Environment, Health, and Natural Resources to protect and
preserve the water and air resources of the State. The Division
of Water Quality has the delegated authority to enforce adopted
pollution control rules. This letter is a standard notification
and is intended to advise you of the legal requirements under
North Carolina law. This notice documents a violation of the
North Carolina groundwater standards as identified in the
Cascaddan water supply well analytical report received on
November 1, 1996.
Specific violations of 15A NCAC 2L .0103(d) -No person
shall conduct or cause to be conducted any activity which causes
the concentration of any substance to exceed that specified in
15A NCAC 2L .0202 -are as follows:
Constituent Concentration* 2L Standard*
Nitrate 11 1 0
* concentration in parts per million
You are responsible for causing, contributing to or allowing
the continuing violation of the underground water quality
standards because you have stored and/or disposed of septage
waste in unlined lagoons.
919 North Moin Street,
Mooresville, North Carolina 28115
Voice 704-663-1699
FAX [phone]
An Equal Opportunity/Affirmative Action Employer
50"k recycled/10"/o post-consumer paper
A.A.A. Enterprises
November 5, 1996
Page 2
15A NCAC 2L .0106(b) states that any person conducting or
controlling an activity which results in the discharge of a
waste, hazardous substance or oil to the groundwater, or in
proximity thereto, shall take immediate action to terminate and
control the discharge, mitigate any hazards resulting from
exposure to the pollutants and notify the Department of the
discharge.
To comply with this section of the rules, you must provide
an alternate drinking water supply for the residents who use the
well at 177 Lauren Drive within seven days of receipt.
In addition, 15A NCAC 2L .0106(f) requires that abatement,
containment or control of the contaminants occur prior to or
concurrent with assessment activities. It has come to our
attention that storage and/or disposal of septage has resumed at
this site under the business name of Sigmon Environmental, Inc.
Please submit a report explaining your procedures for storing and
disposing of septage at this site in a way that does not further
impact the groundwater in this area. This report shall be
received by this office no later than 30 days of receipt of this
letter.
You should be aware that any violation bf 15A NCAC 2L may
subject you to a civil penalty assessment under the authority of
G.S. 143-215.6A of up to $10,000 per rule violation. Each day
that the violation continues may be considered a separate
violation. Failure to respond within the time specified and to
voluntarily achieve compliance may result in a recommendation for
enforcement, the issuance of a Special Order against you under
the authority of G.S. 143-215.2, or a request to the Attorney
General to institute an action for injunctive relief.
Your response and/or questions should be directed to
Paul Dahlen of the Mooresville Regional Office at [phone],
ext. 234.
cc:
Sincerely a
. (__)I i.Ji:::i ... ec~-~-i
B .. ~ith Overcash, P.E.
Re ional Supervisor
.{roundwater Section -
Iredell County Health
Allen Cascaddan
Raleigh
Dept.
Mike James
Enclosures: Lab Results
Toxicological Evaluation
COUNTY
QUAD NO:
!REDELL
RECE\YEO/EHHR C
QHI. GROUHO WATER Sc.C.
. . . DIV.1,)\91>\fJf.!'rVIRONMENTAL MANAGEMENT 96. NOV -S \.,.Qh~Jfury t'11bor11tory llrporl f Ground W111rr Qualily
SAMPLE PRlQRITY
~ROUTINE ~H>1ERGENCY
REPORT TO
COLLECTOR(S)
DATE:
_,_1R_O __________ R..-~donal Office El CHAIN OF CUSTODY
E] SAMPLE TYPE □ D,\IILEN
!Ont<J6
TIME·
PURPOSE·
LABO RA TORY ANALYSIS
BODJl0 mg/L
COD High 340 mg/L
COD LowJJ5 ,mg/L
Coliform: MFFecalJJ616 1100ml
Coliform· MF Total 31504 1100ml
TOC mg/1
Turbility NTU
Residue., Suspended 530 mg/L
fotal Suspended solids mg/L
'
pll 1.11\llS
Alkalini1y 10 pH 4.5 mg/L
Alkalinity to pH 8.3 ' mg/L
Cnrbonate mg/L
Bicarbonate m&fL
Carbon dioxide mg/L
Chloride mg/L
Chromium: Hex I 032 ,g!L
Color: True 80 c.u.
Cyanide 720 mg/L
:OMMENTS:
o,~ncr:
Location or Site:
Description of sampling point
S~mpling Method
Rrniaiks:
Diss. Solids 70300
Fluoride 951
Hardness: total 900
Hardness: (non-crub) 902
Phenols 32730
Sp~ific Cond. 95
Sulfate
Sulfide 745
, MBAS
Oil imJ G1c1ne
Silica
Boron
NHJ as N 610
TKN as N 625
X NO2 +NO3 as n 630
P: Total 11s P 665
ro,
RACHEL BROWN
mg/L Ag-Sih·cr 46566
mg/L Al-Aluminum 46557
mg/L As-Arsenic 46551
m,IL Ba-Barium 46558
,g/L Ca-Calcium 46552
uMhos/cm2 Cd-Cadium 46559
mg/L Ci-Chromium 46560
rng/L Cu• Copper !042
mgll. l'e• lrn11 10·15
mg/L X 111_1-Mcmny 71900
111g/L K-l'otassium 46555
Mg-Magnesium 927
l\ln-Maugnnese 1055
0.02 mg/L Na-Sodium 929
ms'L : Ni-Nickel
7.3 mg/L Pb•Lend 46564
mg.IL Se•Sclcnium
mg/L Zn Zinc 46567
Lab Number 6G2233
Date Recehed I0/!/96
Time Ret:rh·ed 9:30 AM
RcccivW Oy OS
Rclensi:d Dy OS
Date reported ; 11/4196
,,IL Organochlorine Pesticides
,g/L Organophosphorus Pesticides
,g/L Nitrogen Pesticides
,,;'L
mg/L Acid I lerbicides
,g/L
,g/L X Semi,olatiles
,g/L rrll-lJiescl Range
1111/L
5.1 UJ!.11. X \'oln1ile Or1tnnic~ (\'O,\ l>vule)
mg/L
mg/I. J"PII-G~soline Ran1_1e
u11IL I 1'11-BTEX G11solinc Range
mg/L
,g!L
ug/L
ug/1.
,,,L
6G223J.OCT
GROUNDWATER FIELD/L,AB FORM
County -e,d,__ LI
North Catollna
Oeparlment of Environment, Health, ond Natural Resources
DIVISION OF ENVIRONMENTAL MANAGEMENT-GROUNDWATER SECTION
Lab Number ---..,,-:-¥7"--+-""-"''-'-'--~--;:::--=---
ouadNo t..,7n-8 SerialNo_______ SAMPLEPRIORITY 0
Lat. -;i S-, '-t.)... 'S8''N Long. ~8~0-0 =•S~-d-'_i~B-"W __ ]~rROUTINE . fil'EMERGENCY
, ~ . , ._ ; [J91;fAIN,OF QU~l,QDY{'; ff Report To: ARO, FR~ RRO, WaRO, WiRO, ,._; j ii'.!\',] ';_,r ; _ ,,n,n.l l •,/ -
WSRO, Kinston FO, Fed. Trust, Central Off., Other: ________ _
Date Received µ-c.µL.4--'-"-¥'--
Rec·d by:.,[~)kS~--rom: us _____ _d Del.,
Other: ________________ _
Data Entry By: ______ Ck: ______ _
Date Reported: _____________ _
Shipped by: Bus,,9ourieJ( f;land Del., Other_· ___________ _
Collector(s): Yq./2 f e,,.. ,, Date I 4 7 / '1 b . r • FIELD ANALYSES
pH ~s~-5-Spec. Cond.94 400 I Temp.10 /o 0c Odor_·-____ _
Appearance < i..,c.):/c:c.(,c,-u/L
' , I • Field Analysis By: ~-<'-~'-~L<=-~---~----
LABORA TORY ANALYSES
Description of sampling point -='-'-'~=-----------------------
Sampling Method ______ .....,.~---~---------Sample Interval _______ _
~1181,etc) ...--1. _/ · · ( Remarks e '"' /,/t.L. c~..e. v.-, ,..... ~ ~ We c,... ,1t.,(....,)
(pumping lime, a· mp. 111c.)
BOD. 310 mail Diss. Solids 7030□ mntl Aa • Silver 46566 ua/1 Orqanochlorine Pesticides
COD High 340 I mg/I Flouride 951 mnn Al -Aluminum 46557 ua/1 Organophosphorus Pesticides
COD Low335 mg/I Hardness: Total 900 ninl/ As -Arsenic 46551 ua/1 Nilroqen Pesticides
Coliform: MF Fecal 31616 1100ml Hardness tnon-carb) 902 mail Ba -Barium 46558 ua/1
Coliform: MF Total 31504 /100ml Phenols 32730 urn I Ca -Calcium 46552 mail Acid Herbicides
TOG 680 mail ·--...snedfic Cond. 95 uMhos/cm2 Cd• Cadmium 46559 ua/1
Turbidily 76 NTU Sulfate 945 mail Cr -Chromium 465G0 ua/1 '">< Semivolatile Organics
Residue., Suspended 530 mgil Sullide 745 mail Cu • Conner 46562 uail
Fe -hon 46563 Uqil
I>< HQ• Mercury 71900 uq/1 --x Volatile Organics (VOA botlle)
pH 403 units . K • Potassium 46555 mg/I
Alkalinity to pH 4.5 410 mg/1 Ma -Maanesium 46554 ma,I TPH -Gasoline Range
Alkalinily 1o pH 8.3 415 mg/I Mn -Manc:ianese 46565 uq/1 TPH -BTEX Gasoline Range
Carbonate 445 mg/I NH_ as N 610 mail Na -Sodium 46556 ma,I
Bicarbonate 440 mq/l TKN •• N sos __ ,, Ni -Nickel uni!
Carbon dioxide 405 I mq~ 'x NO +NO as N 630 mail Pb -Lead 46564 ua/1 ' <:_
Chloride 940 mg/I P: To1al as P 665 mail Se • Selenium uq/1 \ ' ,./
Chromium: Hex 1032 ug/1 Zn • Zinc 46567 unn '
Color: True 80 Pt-Co '
Cyanide 720 mg/I
Lab Comments:-------~-------------------------------------------------
GW-54 REV. 6'9.1 For Dissolved Analysis -submit filtered sample and write "DIS" in blor.1•
BW~ {foi
EHNRIOEM LABORATORY LAB NO. 6G2233
VOLATILE ANALYTICAL REPORT
REPORTED BY SUPERVISOR
CHECKED BY ~· REVIEWED BY
SAMPLE TYPE. WATER ANALYSIS RESULTS
75-35-4 1, 1-0ichlciroethene 0.75 u 96-18-4 1,2,3-Trichloropropane 0.25 u
75-09-2 Methylene Chloride 10 u 108-86-1 Bromobenzene u . ' 156-60-5 trans-1,2-Dichloroethene 0.75 u 95-49-8 2-Chlorotoluene 0.25 u
75-34-3 1, 1-Dich!oroethane 0.25 0.63 106-43-4 4-Chlorotoluene 0.25 u
590-20-7 2,2-Dichloropropane 0.25 u 541-73-1 1,3-Dichlorobenzene 0.25 u
156-59-4 cis-1,2-Dichloroethene 0.25 0.81 E 106-46-7 1,4-0ichlorobenzene 0.25 0.83
67-66-3 Chloroform 0.25 u 95-50-1 1, 2-Dichlorobenzene 0.25 u
74-97-5 Brornochloromethane 0.75 u 96-12-8 1,2-Dibromo-3-Chloropropane u
71-55-6 1, 1.1-Trichloroethane 0.25 u 120-82-1 1,2,4-Trichlorobenzene 0.25 u
563-58-6 1, 1-Dichloropropene 0.25 u 87-68-3 Hexachlorobutadiene 0.25 u
56-23-5 Carbon Tetrachloride 0.75 u 87-61-6 1,2,3-Trichlorobenzene 0.75 u
107-06-2 1,2-Dichloroethane 0.25 u 1634-04-4 Methyl-tert-butyl ether 5 u
79-01-6 Trich!oroelhene 0,25 D 71-43-2 Benzene u
78-87-5 1,2-Dichloropropane 0.25 u 108-88-3 Toluene u
75-27-4 Bromodichlorornethane 0.25 u 100-41-4 Ethyl benzene 1 u
74-95-3 Dibromomethane 1 u 108-38-3 m,p-Xylenes 2 2.0
10061-01-5 cis-1,3-Dichloropropene 0.25 u 95-47-6 a-Xylene u
10061-02-6 trans-1,3-Dichloropropene 0.25 u 100-42-5 Styrene u
79-00-5 t, 1,2-Trichloroethane 0.25 u 98-82-8 lsopropylbenzene u
127-18-4 T etrachloroethene 0.25 u 103-65-1 n-Propylbenzene u
142-28-9 1,3,-DichloroprJpane 0.25 u 108-67-8 1,3,5-Trimethylbenzene u
124-48-1 Dibromochforornelhane 0.75 u 98-06-6 lert-Butylbenzene u
106-93-4 1.2-Dibromoelhane u 95-63-6 1, 2,4-Trirnethy!benzene u
108-90-7 Cl1lorobenzene 0.25 u 135-98-8 sec-Bulylbenzene u
630-20-6 1, 1, 1,2-Tetra~hloroethane 0.25 u 99-87-6 p-isopropylloluene u
75-25-2 Bromoform 0.5 u 104-51-8 n-Butylbenzene u
79-34-5 1, 1,2,2-Tetrachloroethane 0.75 u 91-20-3 Naphthalene u
.. .. .. • mgfl mg/L
TQL-Target Ouantitation Limit-Subject to Gilsoiin8 R~ng_e Estimated T0tal Petrol8um Hydr~arbon 0.25 N
change due to instrument sel1sitivity
T-Tentatively Identified. not confirmed Other purgeables detected Detected
E-Estimated Value (up to 10 highest peaks) ug/L
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this_ compound TWO UNIDENTIFIED PEAKS DETECTED BY GCfPID.
0-oetected below quantitation limit .
M-GCfMS Analysis pertorrned
COMMENTS•
EHNR/DEM LABORATORY LAB NO. 6G2233
SEMI-VOLATILE ANALYTICAL REPORT
REPORTED BY ·~ SUPERVISOR-r ~
CHECKED BY
REVIEWED BY
DATE 1m;;w,
ENTERED BY
SAMPLE TYPE: WATER 1 ANALYSIS RES UL TS DATE
62-53-3 ANILINE 10 u 606-20-2 2,6-DINITROTOLUENE 10 u
108-95-2 PHENOL 10 u 99-09-2 3-NITAOANILINE 50 u
111-44-4 . 8IS12-CHLOROETHYL) ETHER 10 u 83-32-9 ACENAPHTHENE 10 u
95-57-8 2-CHLOROPHENOL 10 u 51-28-5 2,4-DINITAO PHENOL 50 u
541-73-1 1,3-DICHLOROBENZENE 10 u 100-02-7 4-NITRO PHENOL 50 u
106-46-7 1 ,,4-D!CHLOROBENZENE 10 u 132-64-9 DlBENZOFURAN 10 u
100-51-6 BENZYL ALCOHOL 20 u 121-14-2 2,4-DINITAOTOLUENE 10 u
95-50-1 1,2-DICHLOAOBENZENE 10 u 84-66-2 DIETHYL PHTHALATE 10 u
95-48-7 2-METHYL PHENOL 10 u 7005-72-3 4-CHLOROPHENYL PHENYL ETHER 10 u
108-60-1 BIS(2-CHL□Ro1s□PROPYU ETHER 10 u 86-73-7 FLUORENE 10 u
106-44-5 4-METHYL ,PHENOL 10 u 100-01-6 4-NITROANILINE 50 u
621-64-7 N-NJTROS0-0I-N-PROPYLAMINE 10 u 534-52-1 4,6-DINITR0-2-METHYL PHENOL 50 u
I 67-72-1 HEXACHLOROETHANE 10 u 86-30-6 N-NITROSODIPHENYLAMINE 10 u
98-95-3 NITROBENZENE 10 u 101-55-3 4-BROMOPHENYL PHENYL ETHER 10 u
78-59-1 ISOPHORONE 10 u 118-74-1 HEXACHLOROBENZENE 10 u
88-75-5 2-NITRO PHENOL 10 u 87-86-5 PENT ACHLORO PHENOL 50 u
105-67-9 , 2,4-DIMETHYL PHENOL 10 u 85-01-8 PHENANTHRENE 10 u
65-85-0 BENZOIC ACID 50 u 120-12-7 ANTHAACENE 10 u
111-91-1 8IS(2-CHLOAOETHOXY) METHANE 10 u 84-74-2 DI-N-BUTYL PHTHALA TE 10 u
120-83-2 2,4-0ICHLORO PHENOL 10 u 206-44-0 FLUORANTHENE 10 u
120-82-1 1,2,4-TRICHLOROBENZENE 10 u 129-00-0 PYRENE 10 u
91-20-3 NAPHTHALENE 10 u 85-68-7 BUTYLBENZYL PHTHALATE 10 u
106-47-8 4-CHLOROANlLINE 20 u 91-94-1 3, 3' -OICHLOROBENZIDINE 20 u
87-68-3 HEXAi:HLOROBUTADIENE 10 u 56-55-3 BENZO(A)ANTHRACENE 10 u
59-50-7 4-CHLOR0-3-METHYL PHENOL 20 u 218-01-9 CHRYSENE 10 u
91-57-6 2-METHYL NAPHTHALENE 10 u 117-81-7 BIS(2-ETHYLHEXYLJ PHTHALATE 10 u
77-47-4 HEXACHLOROCYCLOPENT ADI ENE 10 u 117-84-0 0I-N-OCTYL PHTHALATE 10 u
88-06-2 2,4,6-TRJCHLORq PHENOL 10 u 205-99-2 BENZO{B)FLUORANTHENE 10 u
95-95-4 2,4,5-TRICHLORO PHENOL 10 u 207-08-9 BENZO(K)FLUOAANTHENE 10 u
91-58-7 2-CHLORO NAPHTHALENE 10 u 50-32-8 BENZO(AJPYRENE 10 u
88-74-4 2-NITROANILINE 50 u 193-39-5 INDENO( 1,2,3-CD)PYRENE 10 u
131-11-3 DIMETHYL PHTHALATE 10 u 53-70-3 018ENZOIA.HIANTHRACENE 10 u
208-96-8 ACENAPHTHYLENE 10 u 191-24-2 BENZO(G,H,l)PERYLENE 10 u
SEMIVOLATILE ORGANICS REPORT-DEM LAB PAGE 2
UNIDENTIFIED 22E
LAB N0. __ _;.6_G_2_2_;.3_3
TOL-Target Ouantitation limit-Subject to
change due to instrument sensitivity
T-Tentatively Identified, ·estimated concentration
E-Estimated Value
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound
0-Detected below quantitation limit
H-Holding time eXceeded
COMMENTS: _________ _;._ _____________________________________ _
..
COUNTY
QUAD NO:
!REDELL
I\El'ORTTO
COI.LECTOR(S)
ll,\lE:
_,_,_n_o _________ Regionnl Office
DAIi LEN
J!lill!!
llME:
l'URPOSE:
LABORATORY ANALYSIS
DODJI0
COD lligh 340
COD I.ow BS
Coliform: MF fec,1 J\616 -Colifonn: MFT01a1)1504
TOC
Turbitity
Residue., Suspended 530
Total Suspended s.olids
pH
Alkalinity to pH 4.5
Alkalinity to pH 8.J
Carbonate
Bicarbonate
Carbon dio~ide
Chloride
Chromium: lk~ 1032 ~-
rolor: True 80 --l\anide 720
COi\lMENTS:
rng/L
rng/L
mg/L
/1001111
1100ml
rng/1
NTU
rng/L
rng/L
units
rng/L
rng/L
rng/L
rng/L
rng/L
mg/L
,gtL ,,
mgfl.
Owner:
Location or Site:
Description of sampling point
Sampling Method·
Remarks:
Diss. Solids 70)00
Fluoride 951
llmdncss: 1olnl 900
I lnrd11css: (non-carb) 902
rhenob 32730
Specific Cond. 95
Sulfate
Sulfide 745
MBAS
Oil and Grease
Silica
Boron
NIU as N 610
TKN as N 625
N02 +N03 as n 6)0
P: Total as P 665
ro,
DIVISION OF ENVIRONMENTAL MANAGEMENT
Chcmi"ry L•bon1tory Report/ Ground WAIU Qulily
SAMPLE PRIORITY
□ROUTINE
~ CIIAINOFCUSTODY
~ SAMPLE TYPE
DA \'IDSON RENTAi. N2
rng/L
mg.IL
mg/I.
mg/L
,g/L
uMhos/cm2
rng/L
rng/L
rng/L
rng/L
rng/L
rng/L
rng/L
mglL
m11.IL
mg1L,
e)EMERGENCY
□
Ag-Silver 46566
Al-Aluminum 46557
As-Arsenic 46551
Ila-Barium 46558
Ca-Calcium 46552
Cd-Cadium 46559
Cr-Chromium 46560
Cu-Copper 10-U
Fe-Iron 1(µ5
Ilg-Mercury 71900
K-Po1assium 46555
~lg-Magnesium 927
~In-Manganese 1055
Na-Sodium 929
Ni-Nickel
Pb-Lead 46564
Sc-Selenium
Zn_Zinc 46567
'
Lab Number 6G2231
Date Received : 10/8/96
Time Received \ 9:30 AM
Received By OS
Released Dy OS
Date reported : 1on1/96
,giL Organochlorine Pesticides
ug!L Organophosphorus Pesticides
ug/1. Nitrogen Pesticides
ug/L
mg/L Acid I krbicidcs
,g/L
,g/L ' Seml\·o!atilcs
,g/L TPH-Diesel Range
uglL
ug/L ' Volatile Organics {VOA bottle)
rng/L
mg.IL TPH-Gasoline Range
u_[I/L TPH-BTEX Gasoline Range
rng/L
•~L
,g/L
ug/L
uglL
6G22J1.0CT
Nor I h Carol Ina I GROUNDWATER FIELD/LAB FORM
;OLL.: ,,J J' I-~
/2,ruf(
Depattmenl of Environment, Health, and Natural Resources
DIVISION OF ENVIRONMENTAL MANAGEMENT-GROUNDWATER SECTION
County _ _.-,-=,_,j_""'-'"-'/ /,__ ________ _
Quad No L. 6 7 'l iJ Serial No.--~----
Lat. 3~-":t.2.1 r['IJJ Long. !Jc/•:,-8 '1,l. '11.J
lleport To: ARO, FRO~. ARO, WaRO, WiRO,
SAMPLE PRIORITY
□ROUTINE ~EMERGENCY
~CHAIN OF CUSTODY
Shipped by: Bus, Courie , Hand Del., Other· _ ),_ i! U,
0 Date Reported: _____________ _
WSRO, Kinston FO~_._E. Trust, Central Off., Other: ___ ~1 _~~-~ .. ~~~~,-....,Jr--;f\lR-'CF, -CUSTODY
.I I , • · Purpose: ----:-:,
Collector(s): Usli 4 Date / 6/ 7 / '[L Time / ,,_-3 ° Baseline1 Complain Compliance, LUST, Peslicide Study, Federal Trust, Other:
[IELD ANALYSES r r . 0 owner '"'"
00001 I,, _b~:£"1...__i?,_,;;:h::t:::1!:..2-~-__.:._____: _____________ _
Jo at25o c Location or site _.t.,1!:,'._L!--o,;;;.,deu~<'L:'._ ______ -, ________________ _
Description of sampling point --~=;~·"''c;_,'fc:D"-{.,_..,,,,~_,1,"-,.~«...,,_l_,c~.Ft::-'h=a..~· k:5--"--"~--------------
Sampling Method --------,,e.Q.;::....-4_',_,-.. -,.,-"-
1
________ Sample lnterval _______ -'---
Remarks e--l -1-.. )-,.,.., i
pH,00 •,-., -·J..d Spec. Cond.9,
Temp.10 / B °C Odor _.L,,z,.,t"''"'v>--::::.... __ _
Appearance G Gv.-..-Jc, { ,_ (,,__,,.,,
Field Analysis By: --~J.,J=J.£.=--------(pumping lim,, air tamp. elc.)
LABORA TORY ANALYSES
BOD. 310 mall Diss. Solids 70300 mn•I An -Silver 46566 uall Oraanochlorine Pesticides
COD High 340 mg/I Flouride 951 mnn Al -Aluminum 46557 uatl Organophosphorus Pesticides
COD Low 335 mail Hardness: Total 900 mnll As. Arsenic 46551 unll Nifroqen Pesticides
Coliform: MF Fecal 31616 1100ml Hardness lnon-carbl 902 mnll Ba -Barium 46558 ua/1 ,
Coliform: MF Total 31504 1100ml Phenols 32730 u-• Ca . Calcium 46552 mn/1 Acid Herbicides
TOC 680 mnil Snecific Cond. 95 uMhos/cm2 Cd • Cadmium 46559 uatl
Turbidity 76 NTU Sulfate 945 mn!I Cr -Chromium 46560 uall X: Semivolatile Organics
Residue., Suspended 530 mg/I Sulfide 745 mail Cu . Conner 46562 ua/1
Fe• Iron 46563 ua/1
Ha• Mercury 71900 ua/1 ~ Volatile Organics (VOA bottle)
pH 403 units K -Potassium 46555 mail
Alkalinity to pH 4.5 4to mg/I Mn . Maanesium 46554 ma/I TPH -Gasoline Range
Alkalinity to pH 8.3 415 mg/I Mn -Man□anese 46565 ua/1 TPH -BTEX Gasoline Range
Carbonate 445 mgtl NH as N Gto mail Na • Sodium 46556 ma/I
Bicarbonate 440 mn/1 Il$t:l as t:l 620 mgll.. Ni -Nickel unll I ~
Carbon dioxide 405 mg/I NO + NO. as N 630 mnll Pb -Lead 46564 un!I ,I I )
Chloride 940 mg/I P: Total as P 665 mnil Se -Selenium uatl " I
Chromium: Hex 1032 unn Zn -Zinc 46567 unn
Color: True 80 Pt-Co '
Cyanide 720 mg/I
Lab Comments: ----------------------------------------------
GW-54 REV. 619:'l For Dissolved Analysis -submit filtered sample and write "01S" in bier' ·-
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
62-53-3
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-76-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-B
87-6B-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
WATER
ANILINE
PHENOL
815(2-CHLOAOETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-0ICHLOROBENZENE
BENZYL ALCOHOL
1,2-0ICHLOROBENZENE
2-METHYL PHENOL
BIS(2-CIILOROISOPROPYL) ETHER
4-METHYL PHENOL
N-NITROS0-01-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITRO PHENOL
2,4-DIMETHYL PHENOL
BENZOIC ACID
BIS(2-CHLOROETHOXY) METHANE
2,4-0ICHLORO PHENOL
1.2.4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUT ADIENE
4-CHLOR0-3-METHYL PHENOL
2-METHYL NAPHTHALENE
HEXACHLOROCYCLOPENT ADI ENE
2,4,6-TAICHLOAO PHENOL
2,4,5-TAICHLORO PHENOL
2-CHLOAO NAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
EHNR/DEM LABORATORY
SEMI-VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
10 u 606-20-2
10 u 99-09-2
10 u 83-32-9
10 u 51-28-5
10 u 100-02-7
10 u 132-64-9
20 u 121-14-2
10 u 84-66-2
10 u 7005-72-3
10 u 86-73-7
10 u 100-01-6
10 u 534-52-1
10 u 86-30-6
10 u 101-55-3
10 u 118-74-1
10 u 87-86-5
10 u 85-01-8
50 u 120-12-7
10 u 84-74-2
10 u 206-44-0
10 u 129-00-0
10 u 85-68-7
20 u 91-94-1
10 u 56-55-3
20 u 218-01-9
10 u 117-81-7
10 u 117-84-0
10 u 205-99-2
10 u 207-08-9
10 u 50-32-8
50 u 193-39-5
10 u 53-70-3
10 u 191-24-2
2,6-DINITROTOLUENE
3-NITROANIUNE
ACENAPHTHENE
2,4-0INITRO PHENOL
4-NITRO PHENOL
DIBENZOFURAN
2,4-0INITROTOLUENE
DIETHYL PHTHALATE
4-CHLOROPHENYL PHENYL ETHER
FLUOAENE
4-NITROANIUNE
4,6-DINITR0-2-METHYL PHENOL
N-NITROSODIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE
PENT ACHLORO PHENOL
PHENANTHRENE
ANTHRACENE
Df-N-BUTYL PHTHALATE
FLUORANTHENE
PYRENE
BUTYLBENZYL PHTHALATE
3, 3 '-DICHLOROBENZIDINE
BENZO(A)ANTHAACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
Dl-N-OCTYL PHTHALATE
BENZO(B)FLUORANTHENE
BENZO(K)FLUORANTHENE
BENZO(A)PYRENE
INDENO(l ,2,3-CD)PYAENE
DIBENZO(A,H)ANTHAACENE
BENZO{G,H,l)PERYLENE
LAB NO. 6G2231
10
50
10
50
50
10
10
10
10
10
50
50
10
10
10
50
10
10
10
10
10
10
20
10
10
10
10
10
10
10
10
10
10
J _,
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
SEMIVOLATILE ORGANICS REPORT -DEM LAB PAGE 2 LAB NO. __ 6=..G::.;2::.;2:;.:3c;..1
NO BASE/NEUTRAL OR ACID EXTRACT ABLE ORGANICS
DETECTED BY GC/MS. ___________ ~To~-~-u-~~w
change due to instrument sensitivity
T-Tentatively Identified, estimated concentration
E-Estimated Value
U-Samples analyzed for this compound but not detected·
N-Sample not analyzed for this compound
0-Detected below quantitation limit
H-Holding time exceeded
COMMENTS:----------------------------------------------------
EHNR/DEM LABORATORY
LAB NO. 6G2231
~ VOLATILE ANALYTICAL REPORT
REPORTED BY SUPERV~~~: S~o; 91;;, (//(!__,
CHECKED BY
REVIEWED BY ENTERED BY
SAMPLE TYPE: WATER ANALYSIS RESULTS DATE I () j (,2
75-35-4 1, 1-Dichloroethene 0.75 u 96-18-4 1,2,3-Trich!oropropane 0.25 u
75-09-2 Methylene Chloride 10 u 108-86-1 Bromobenzene 1 u
156-60-5 lrans-1,2-0ichloroethene 0.75 u 95-49-8 2-Chlorotoluene 0.25 u
75-34-3 1. 1-Dichloroelhane 0.25 u 106-43-4 4-Chlorotoluene 0.25 u
590-20-7 2. 2-Dich1oropropane 0.25 u 541-73-1 1,3-Dichlorobenzene 0.25 u
156-59-4 cis-1,2-Dichloroethene 0.25 u 106-46-7 1. 4-0ichlorobenzene 0.25 u
67-66-3 Chloroform 0.25 u 95-50-1 1,2-Dichlorobenzene 0.25 u
74-97-5 Bromochloromethane 0.75 u 96-12-8 1. 2-Dibromo-3-Chloropropane
u
71-55-6 1, 1, 1-Trichloroethane 0.25 u 120-82-1 1,2,4-T richlorobenzene 0.25 u
563-58-6 1, 1-Dichloropropene 0.25 u 87-68-3 Hexachlorobutadiene 0.25 u
56-23-5 Carbon Tetrachloride 0.75 u 87-61-6 1,2,3-T rich!orobenzene 0.75 u
107-06-2 1, 2-Dichloroethane 0.25 u 1634-04-4 Methyl-tert-butyl ether 5 u
79-01-6 Trichloroelhene 0.25 u 71-43-2 Benzene u
78-87-5 1,2-Dichloropropane 0.25 u 108-88-3 Toluene u
75-27-4 Bromodichloromelhane 0.25 u 100-41-4 Ethyl benzene 1 u
74-95-3 Oibromomethane
u 108-38-3 m,p-Xylenes 2 u
10061-01-5 cis-1,3-0ichloropropene 0.25 u 95-47-6 a-Xylene
u
10061-02-6 trans-1,3-Dichloropropene 0.25 u 100-42-5 Styrene
u
79-00-5 1, 1,2-Trichloroethane 0.25 u 98-82-8 lsopropylbenzene
u
127-18-4 Tetrach1oroethene 0.25 u 103-65-1 n-Propy!benzene u
142-28-9 1,3-Dichloropropane 0.25 u 108-67-8 1, 3, 5-T rimethylbenzene u
124~8-1 Oibromoch1oromethane 0.75 u 98-06-6 tert-Butylbenzene u
106-93-4 1, 2-Dibromoethane u 95-63-6 1,2,4-Trimethylbenzene
u
108-90-7 Chlorobenzene 0.25 u 135-98-8 sec-Butyl benzene u
630-20-6 1, 1.1,2-Tetrachloroethane q.25 u 99-87-6 p-isopropyltoluene u
75-25-2 Bromoform 0.5 u 104-51-8 n-Butylbenzene u
79-34-5 1, 1,2,2-Telrachloroelhane 0.75 u 91-20-3 Naphthalene
u
mgll mg/L
TOL-Targel Ouantitation Limit-Subject lo Gasoline Range Estimated Total Petroleum Hydrocarbon 0.25 N
change due to instrument sensitivity
T-Tentatively Identified, not confirmed Other purgeables detected Detected
E-Estimated ValuE? (up to 10 highest peaks)
ug/L
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for lhis compound NO VOLATILE ORGANIC COMPOUNDS DETECTED BY
0-Detected below quantitation limit GC/ELCD.
M-GC/MS Analysis performed ONE UNIDENTIFIED PEAK DETECTED BY GC/PID.
COMMENTS:
COUNTY ·
tJUAO NO:
!REDELL
r.r:rORTTO
(OI.LECTOR(SJ
l>AlE·
-~c~-•",~"L'E"N~-------Regional Office
10/7196
·1rME:
ruRrOSE:
LABORATORY ANALYSIS
800310
COO lligh 340
COO low BS
Coliform: MF Fecal 31616
Coliform: MF Total J\504
TOC
Turbitity
Residue .• Suspended S30
Total Suspended solids
pll
Alkalinity to pll 4.S
Alkalinity to pH 8.3
Carbonate
Bicarbonate
Carbon dio:itide
Chloride
Chromium: lie:,; 1032
Color: True 80
Cyanide 720
COMMENTS:
mg/L
mg/L
mg/L
1100ml
/IOOml
mg/1
NTU
mg/L
mg/L
units
mg/L
mg/L
mg/L
m•'L
mg/L
mg/L
ug/1.
"
111g1L
o,,ner.
Local ion or Site:
Oesc,iplion of sampling point
Sampling Method:
Remru-ks·
Diss Solids 70300
Fluoride 951
Hardness: total 900
I loidness: (non-carb) 902
Phenols 32730
Specific Cond. 95
Sulfa1e
Sulfide 745
MBAS
Oil end Gre:rn:
Silica
Boron
NH3asN610
TKN as N 625
N02 +NOJ as n 6)0
P· Total as P 665
ro,
DIVISION OF EN\'lnONI\IENTAL I\IANAGEi\fENT
Cht-mistry L•bonlory Report I Ground \\'•In Qu.lily
SAMPLE PRIORITY
□ROUTINE
E) CIIAINOFCUSTODY
E] SAMPLE TYPE
OA\'IDSON RENTAL 111
mg/L
mg/L
mg/L
mg/L
,g/L
uMhoslcm2
mg/L
mg/L
mg/I.
mg/I.
mg/L
m•'L
mg/L
mg}L
mg/I.
mg/L
~Ef,,IERGENCY
□
Ag-Silver 46566
Al-Aluminum 46557
As-Arsenic 46551
Ba•B.11ium 46558
Ce•Colcium 46552
Cd·Cadium 46559
Cr-Chromium 46560
Cu• Copper I 042
Fe-Iron I0-15
Hg-Me,cury 71900
K-Potassium 46555
Mg-Magnesium 927
Mn-Manganese 1055
Na-Sodium 929
Ni-Nickel
Pb•Lcad 465~
Se-Selenium
Zn Zinc 4656 7
,g/L
ug/L
,g/L
ug/L
mg/L
,g/L
,g/L
ug/L
,gtL
,g/L
mg/L
mg/L
,g/L
mg/L
,g/L
ug)L
ug/L
ugiL
Lab Number 6G2230
Date Recei,·ed 10/8196
Time Received 9:JOAM
Received By DS
Released By DS
Date repo11ed : 10121/96
Organochlorine Pesticides
Oiganophosphorus Pes1icides
Nitrogen Pesticides
Acid I lerbicides
X Semivolatiles
TPII-Die~I Range
' Volatile Organics (VOA bol11e)
Tl'\1-Gasoline Range
TPH·BTEX Gasoline Range
-
6G22l0.0CT
North Carolina
GROUNDWATER FIELD/LAB FORM
Department of Environment, Health, end Natural Resources
DIVISION OF ENVIRONMENTAL MANAGEMENT-GROUNDWATER SECTION
County ::;:-ecfL{,,/
Quad No '-G 7,,.., ,,_ Serial No.______ SAMPLE PRIORITY 0
Lat .J s-v 'i ;1....t F'i %; Long eo O _; c:' CJ/ '( {.J rv, □ROUTINE qEMERGENCY
· ,.,---:i _@CHAIN OF CUSTODY
neport To: ARO, FRO:--MOO, ARO, WaRO, WiRO, I
WSRO, Kinston FO, Fed. Trust, Central Off., Other: ~ H Al N Q F CU ST(} DY
Shipped by: Bus,~. Hand Del., Other· ___________ _
Lab Number (g_ G 2,J..30 -,
Date Received 16\%\ctG Time, ~~:c..,.,::a=.._
Rec'd by: :r:::f3 From: Bus, ourier
Other: ______________ _
Data Entry By: ______ Ck: ~----
Date Reported: ___________ _
, ( .I . .-Purpose:~ Collector(s): ,J.Kl I.e.,, Date I u~7~''1(.., Time Io:/:, Baseline Complain Compliance, LUST, Pesticide Study. Federal Trust, Other: _____ _ ';'-.... :a_ 1cnclo one)
DELO ANALYSES ff/ Owner Uc:v,dsc,-, l,e,,fd I
rH,00 ~ $--a Spec. Cond.94 >~-al.,18" C Location or site .__...,J v-.
Temp.
10
I 8 _ 0 c Odor_.,,,""""';"''-"--=----Description of sampling point ~t? 'J",,,i •:i l•c. de cf l,u,p
Appearance d.,.,,,f,c·l)1,, t,J/ Sampling Method ,?C;'> Sample Interval ______ _ r ( ci§iiii,ba1kH, olc)
Field Analysis By: c. .,_ <...-.. Remarks _..'c{.s..J'--'-"=='-~-1_.Mic•~"-'-· ----==~~=~C7'---'---------------1Pump1n,;i hmo, air tomp. 01c.)
LABORATORY ANALYSES
BOD. 310 mail Diss. Solids 70300 mnll An • Silver 46566 uall Orqanochlorine Pesticides
COD High 340 mg/I Flouride 951 mall Al -Aluminum 46557 ua/1 Organophosphorus Pesticides
COD Low 335 mg/I Hardness: Total 900 mnll As -Arsenic 46551 ua/1 Nitroaen Pesticides
Colilorm: MF Fecal 31616 1100ml Hardness (non-carbl 902 mnil Ba -Barium 46558 uall
Coliform: MF Total 31504 1100ml Phenols 32730 un,1 Ca -Calcium 46552 mn/1 Acid Herbicides
TOC 680 mall Sgecific Cond. 95 uMhos/cm2 Cd -Cadmium 46559 unll
Turbidity 76 NTU Sulfate 945 mnll Cr -Chromium 46560 ua/1 >< Semivolatile Organics
Residue., Suspended 530 mg/I Sulfide 745 mall Cu . Conner 46562 ua/1
Fe -Iron 46563 uall
Ha -Mercurv 71900 · uq/1 X Volatile Organics (VOA bottle)
pH 403 units K -Polassium 46555 mg/I
Alkalinity to pH 4.5 410 mg/I Ma -Moqnesium 46554 ma/I TPH • Gasoline Range
Alkalinity to pH 8.3 415 mg/I Mn -Manaanese 46565 uq/1 TPH · BTEX Gasoline Range
Carbonate 445 mg/I NH as N 610 mail Na -Sodium 46556 mq/1
Bicarbonate 440 mnn TKN --N r"'5 rngLI Ni -Nickel unil
Carbon dioxide 405 mail NO +NO as N 630 m~• Pb · Lead 46564 un/1 '\ -z::::;-
Chloride 940 mg/I P: Total as P 665 mnll Se -Selenium ua/1 \ I --
Chromium: Hex 1032 unil Zn -Zinc 46567 ua/1
Color: True 80 Pt-Co '
Cyanide 720 mgn
I.ab Comments:-----------------------------------------------------
GW-54 REV. &'93 For Dissolved Analysis -submit filtered sample and write "DIS" in blocl--
EHNR/DEM LABORATORY LAB NO. 6G2230
if_
SEMI-VOLATILE ANALYTICAL REPORT
REPORTED BY SUPERVISOR
CHECKED BY DATE
REVIEWED BY !2'71J ENTERED BY
SAMPLE TYPE: WATER ANALYSIS RESULTS DATE
62-53-3 ANILINE 10 u 606-20-2 2,6-DINITAOTOLUENE 10 u
108-95-2 PHENOL 10 u 99-09-2 3-NITROANIUNE 50 u
111-44-4 BIS(2-CHLOROETHYL) ETHER 10 u 83-32-9 ACENAPHTHENE 10 u
95-57-8 2-CHLOROPHENOL 10 u 51-28-5 2,4-DINITRO PHENOL 50 u
541-73-1 1,3-0ICHLOROBENZENE 10 u 100-02-7 4-NITAO PHENOL 50 u
106-46-7 1.4-DICHLOROBENZENE 10 u 132-64-9 DIBENZOFURAN 10 u
100-51-6 BENZYL ALCOHOL 20 u 121-14-2 2,4-DINITROTOLUENE 10 u
95-50-1 1,2-DlCHLOROBENZENE 10 u 84-66-2 DIETHYL PHTHALATE 10 u
95-48-7 2-METHYL PHENOL 10 u 7005-72-3 4-CHLOROPHENYL PHENYL ETHER 10 u
108-60-1 815(2-CHLOROtSOPROPYL) ETHER 10 u 86-73-7 FLUORENE 10 u
106-44-5 4-METHYL PHENOL 10 u 100-01-6 4-NITROANlllt-!E 50 u
621-64-7 N-NlTROS0-0I-N-PROPYLAMINE 10 u 534-52-1 4,6-DINITR0-2-METHYL PHENOL 50 u
67-72-1 HEXACHLOROETHANE 10 u 86-30-6 N-NITROSOOIPHENYLAMINE 10 u
98-95-3 NlTROBENZENE 10 u 101-55-3 4-BROMOPHENYL PHENYL ETHER 10 u
78-59-1 ISO PHO RONE 10 u 118-74-1 HEXACHLOROBENZENE 10 u
88-75-5 2-NITRO PHENOL 10 u 87-86-5 PENT ACHLORO PHENOL 50 u
105-67-9 2,4-DIMETHYL PHENOL 10 u 85-01-8 PHENANTHRENE 10 u
65-85-0 BENZOIC ACID 50 u 120-12-7 ANTHRACENE 10 u
111-91-1 81S{2-CHLOROETHOXY) METHANE 10 u 84-74-2 0I-N-BUTYL PHTHALATE 10 u
120-83-2 2,4-DICHLORO PHENOL 10 u 206-44-0 FLUORANTHENE 10 u
120-82-1 1,2.4-TRICHLOROBENZENE 10 u 129-00-0 PYRENE 10 u
91-20-3 NAPHTHALENE 10 u 85-68-7 BUTYLBENZYL PH TH ALA TE 10 u
106-47-8 4-CHLOAOANIUNE 20 u 91-94-1 3, 3' -OICHLOROBENZlDINE 20 u
87-68-3 HEXACHLOROBUT ADI ENE 10 u 56-55-3 BENZO(A)ANTHRACENE 10 u
59•50-7 4-CHLOR0-3-METHYL PHENOL 20 u 218-01-9 CHRYSENE 10 u
91-57-6 2-METHYL NAPHTHALENE 10 u 117-81-7 BIS(2-ETHYLHEXYU PHTHALATE 10 u
77-47-4 HEXACHLOROCYCLOPENT ADIENE 10 u 117-84-0 DI-N-OCTYL PHTHALATE 10 u
88-06-2 2.4,6-TRICHLORO PHENOL 10 u 205-99-2 BENZO{B)FLUORANTHENE 10 u
95-95-4 2.4,5-TRICHLORO PHENOL 10 u 207-08-9 BENZO(K)FLUORANTHENE 10 u
91-58-7 2-CHLORO NAPHTHALENE 10 u 50-32-8 BENZO{A)PYRENE 10 u
88-74-4 2-NITROANILINE 50 u 193-39-5 INDENO( 1 ,2,3-CD)PYRENE_ 10 u
131-11-3 DIMETHYL PHTHALATE 10 u 53-70-3 DIBENZO(A,HJANTHAACENE 10 u
208-96-8 ACENAPI ITI IYLENE 10 u 191-24-2 BENZO(G,H,l)PERYLENE 10 u
SEMIVOLATILE ORGANICS REPORT -DEM LAB PAGE 2
NO BASE/NEUTRAL OR ACID EXTRACT ABLE ORGANICS
DETECTED BY GC/MS.
---------
LAB NO. 6G2230 -------
TOL-Target Ouantitation limit-Subject to
ch an g e due to instrument sensitivity
T-Tentatively Identified, estimated concentration
E-Estimated Value
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound
D-Detected below quantitation limit
H-Holding time exceeded
COMMENTS: _______________________________________________ _
I ___,.
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
75-35-4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-16-4
142-26-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79-34-5
TOL-
T-
E-
U-
N-
0-
M-
COMMENTS:
WATER
1, 1-Dichloroethene 0.75
Methylene Chloride 10
trans-1, 2-Dichloroethene 0.75
1, 1-0ichloroe\hane 0.25
2,2-0ichloropropane 0.25
cis-1,2-Dichtoroethene 0.25
Chloroform 0.25
Bromochloromethane 0.75
1, 1, 1-Trichloroethane 0.25
1, 1-0ichloropropene 0.25
Carbon T etrach1oride 0.75
1.2-Dichloroethane 0.25
T rich!oroethene 0.25
1, 2-0ichloropropane 0.25
Bromodichloromethane 0.25
Oibromomethane
cis-1,3-0ich1oropropene 0.25
trans-1,3-Dichloropropene 0.25
1, 1,2-Trichloroethane 0.25
T etrachloroelhene 0.25
1,3-Dichloropropane 0.25
Oibromochloromethane 0.75
1,2-0ibromoethane 1
Chlorobenzene 0.25
1, 1, 1,2-Tetrachloroethane 0.25
Bromofonn 0.5
1, 1,2,2-Tetrachloroethane 0.75
Target Ouanlitalion limit-Subject to
change due to instrument sensitivity
Tentatively Identified, not confirmed
Estimated Value
Samples analyzed for this compound but not detected
Sample not analyzed for this compound
Detected below quantitation limit
GCIMS Analysis performed
EHNRIDEM LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 96-18-4 1,2,3-T richloropropane
u 108-86-1 Bromobenzene
u 95-49-8 2-Chlorotoluene
u 106-43-4 4-Chlorotoluene
u 541-73-1 1,3-Dichlorobenzene
u 106-46-7 1,4-0ichlorobenzene
u 95-50-1 1,2-Dichlorobenzene
u 96-12-8 1,2-Dibromo-3-Chloropropane
u 120-82-1 1,2,4-T richlorobenzene
u 87-68-3 Hexachlorobutadiene
u 87-61-6 1,2,3-Trichlorobenzene
u 1634-04-4 Methyl-tert-butyl ether
u 71-43-2 Benzene
u 108-88-3 Toluene
u 100-41-4 Ethyl benzene
u 108-38-3 m,p-Xylenes
u 95-47-6 o-Xytene
u 100-42-5 Styrene
u 98-82-8 lsopropylbenzene
u 103-65-1 n-Propylbenzene
u 108-67-6 1,3,5-T rimethylbenzene
u 98-06-6 tert-Butylbenzene
u 95-63-6 1,2,4-Trimethylbenzene
u 135-98-8 sec-Butylbenzene
u 99-87-6 p-isopropyltoluene
u 104-51-8 n-Butylbenzene
u 91-20-3 Naphthalene
Gasoline Range Estima!ed Total Petroleum Hydrocarbon
Other purgeab1es detected
(up to 10 highest peaks)
NO VOLATILE ORGANIC COMPOUNDS
DETECTED BY GCIELCDIPID.
LAB NO. 6G2230
SUPERVISOR tfG" t:!. Q,1<2....
DATE !if p/<j~
ENTERED BY ~
DATE ID)IDfJI,
0,25 u
u
0.25 u
0.25 u
0.25 u
0.25 u
0.25 u
u
0.25 u
0.25 u
0.75 u
5 u
u
u
1 u
2 u
u
u
u
u
u
u
u
u
u
u
u
mgfl mgfl
0.25 N
Detected
ugfl
COUNTY
QUAD NO:
IREDELL
. '" '.;_!,' s1:_c.
RErORT TO _,01R0oc_ _________ Regional Office
COLLECTOR(S) : ~D~A~ll~L~E~N-_____ _
DA 1 E: 9n6/96
TIME:
rtJRPOSE:
LABORATORY ANALYSIS
BOD310
COD High340
COD LowJJS
Coliform: MF Fecal 31616
Coliform: MFTotalll504
TOC
Tu,bitity
Residue., Suspended 530
Total Suspended solids
p!l
Alkalinity lo pH 4.S
Alkalinity 10 pH 8J
Carbonate
Bicubona1c
Cmbon dioxide
Chloride
Chromium: lie:,: I0J2
Color: True 80
Cy11nide 720
COMMENTS:
mg/L
mg/L
mg/L
1100ml
/IOOml
mg/I
NTU
mg/L
mg/L
units
mg/L
mg/L
mg/L
m,JL
mg/L
mg/L
,g/L
c.u,
mg/L
O"ner.
l.oeation or Si1c:
Desc:ription of sampling point
Sampling Mcihod
Remarks:
Diss. Solids 70)00
Fluoride 951
I la,dness: total 900
I lardness: (non-carb) 902
Phenols J27J0
Specific Cond. 95
Sulfate
Sulfide 745
MBAS
Oil and Gre,ne
Silica
Boron
NHJ as N 610
TKN as N 625
NO2 +NOJ as n 630
r. Total as r 665
rm
l>l\'ISION OF ENVlltONl\lENTAL l\lANAGE!\IENT
Chemistry L11boralory Rrporl lGro11nd \\'111u Quality
SAMPLE PRIORITY
~ROUTINE
E] CHAIN OF CUSTODY
~ SAMrLE TYPE
CflltlS\\-'
mg/L
mg/L
mg/L
mglL
,g/L
uMhos/cm2
mg/L
mg/L
mg/L
mg/L
mglL
mg/L
mg/L
ms'L
mglL
mg/I.
Oer-.tERGENCY
□
Ag-Silver 46566
Al-Aluminum 46557
As-Arsenic 46551
Ba-Barium 46558
Ca-Calcium 46552
Cd-Cadium 46559
Cr-Chromium 46560
Cu• Copper I 042
Fe• Iron 1{M5
I lg· Mercury 71900
K-ro1assium 46555
Mg-Magnesium 927
Mn-Manganese 1055
Na· Sodium 929
Ni-Nickel
Pb-Lead 465~
Sc-Selenium
Zn_linc -16567
Lab Number 6G2099
Date Reeci,·cd 9127/96
Time Rccei,·ed 9:00AM
Recch·ed By DS
Released By DS
Date reported : 10/14/96
,g/L Organochlorinc Pesticides
,g/L Organophosphorus Pesticides
,giL Nitrogen Pesticides
,g/L
mg/L Acid Herbicides
,,JL
,,JL X Semivolati1cs
,,JL TPH-Oiescl Range
,g/L
,g/L Volatile Organics(VOA boule)
mg/L
mg/L TPH-Gasoline Range
,g/L TPH-BTEX Gasoline Range
mg/L
,g/L ..
,,JL
ugll
uglL
602099 SEP
GROUNDWATER FIELD/LAB FORM
Counly --.;,, ,4. \L
Quad No lr,;J n'.1 Serial No. ______ _
Lat. 3.:[' 4J./ S7''N Long. 8v0 j~~' u] '•u
Report To: ARO, FR~RRO, WaRO, WiRO,
WSRO, l(inslon FO,,_Ee((Trusl, Cenlral Off., OIiier:
V
SAMPLE PRIORITY
flnoUTINE □EMERGENCY
~CHAIN OF CUSTODY
Shipped by: Bus, ~Hand Del., Olher· ___________ _
Norlh C.:atolina
Department of Environment, Health, and Natural Resources
SION OF ENVIRONMENTAL MANAGEMENT· GROUNDWATER SECTION
0
Lab Number l./j;(2,.~099 ·
Date Rec~\';::}_"J (o Time q.'OQ .
Rec"d by:_lJ::)..._.,_"'---rom: Bus@our; Hand Del.,
Olher:
Data Entry By: ______ Ck: ______ _
Date Reported: _____________ _
Purpose:
Colleclor(s): J)d,,.(..._,,., Dale 7 /1t,,/"il. Time _o~'f~:~>_"7.,_ ___ Baseline, omplainl, ornpliance')LUST. Pesticide Study, Federal Trust, Other: ______ _
FIELD ANALYSES r I ' ---C ""''"·' .·
_____ ________ Owner Cbr:/, LJc:,,,~i(~...,,,~~c\ 1
pt-1,00 'f.:, -:;·.o Spec. Cond.9, 't s-at~ C Location or site /7 l C.,-"n?.,,., ~n✓-Wcl( .,.
Temp.,o Z..{ 0 c Odor _s,..,{..,·r4""';}'5---Description of sampling point 5,e,jA CC ,,J,, < f ~
Appearance c (,cc (f: l•~ ~if Sampling Method -------r--===.--------Sample Interval _______ _
/ ~b;ul111,a1c)
Field Analysis By: (..I....,__ Remarks __,u...L-="----l..-",.,,,~--~-=-----===.,.,,=c-=c.-----------------
LABORATORY ANALYSES (p,mpOgtimo.,i<tomp. '"·'
BOD, 310 mg/I Diss. Solids 70300 mg/I Aq • Silver 46566 uq/l Organochlorine Pesticides
COD High 340 mg/I Flouride 95 I mg/\· Ill. Aluminum 46557 uq/l Organophosphorus Pesticides
COD Low 335 mg/I Hardness: Total 900 mg/I As -Arsenic 4655 I ua/I Nitrogen Peslicides
Colilorm: MF Fecal 31616 1100ml Hardness {non-carb} 902 mg/I Ba • Barium 46558 ug/1
Colilorm: MF Total 31504 1100ml Phenols 32730 ug,1 Ca • Calcium 46552 ma/I Acid Herbicides
TOG 680 mg/I _§gecilic Cond. 95 --uMhos/cm2 Cd• Cadmium 46559 ua/1
T urbiditl 76 NTU Sullale 945 mg/I Cr• Chromium 46560 uq/1 ~ Semivolatile Orqanics
Residue., Suspended 530 mg/I Cu • Conner 46562 uq/l
,
Sullide 745 mg/I
Fe -Iron 46563 ug/I
Hg -Mercurt 71900 ug/1 Volatile Organics (VOA botlle)
pH 403 unit~ K . Polassium 46555 mg/I
· Alkalinity lo pH 4.5 410 mg/I Mg • Magnesium 46554 mg/_l TPH • Gasoline Range
Alkalinity lo pH 8.3 415 mg/I Mn • Manganese 46565 ug/1 TPH · BTEX Gasoline Range
Carbonale 445 mg/I NH, as N 610 mg/I Na• Sodium 46556 mq/1
Bicarbonate 440 mg/I .llitLas..N 625 ml)IL Ni -Nickel ug/1 s --
Carbon dioxide 405 mq/1 NO, + NO, as N 630 mg/I Pb. Lead 46564 ug/I ----
Chloride 940 mg/I P: Total as P 665 mg/I Se -Selenium UQ/1
Chromium: Hex 1032 ug/I Zn • Zinc 46567 uq/1
Color: True eo Pt-Co
Cyanide 720 mg/I
Lab Comments: ----------------------------------------------------------
•.. ···--······-·•··-·--·-·--··--··--·----· ··-···-···-···-··---·-···----------·--·
GW-54 REV. 6193 For Uissolvec.J Analysis -subrnil lilterc<l sample and write "UIS" in block.
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
62-53-3
10B-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-98-8
WATER
ANILINE 10
PHENOL 10
BIS(2-CHLOROETHYLl ETHER 10
2-CHLOROPHENOL 10
1,3-DICHLOROBENZENE 10
1.4-DICHLOROBENZENE 10
BENZYL ALCOHOL 20
1,2-DICHLOROBENZENE 10
2-METHYL PHENOL 10
BIS(2-CHLOROISOPROPYL} ETHER 10
4-METHYL Pl--!ENOL 10
N-NITROS0-0I-N-PROPYLAMlNE 10
HEXACHLOROETHANE 10
NITROBENZENE 10
ISOPHORONE 10
2-NlTRO PHENOL 10
2,4-0IMETHYL PHENOL 10
BENZOIC ACID 50
B\S12-CHLOROETHOXYJ METHANE 10
2.4-DICHLORO PHENOL 10
1.2.4-TRICHLOROBENZENE 10
NAPHTHALENE 10
4-CHLOAOANILINE 20
HEXACHLOROBUT ADI ENE 10
4-CHLOR0-3-METHYL PHENOL 20
2-METHYL NAPHTHALENE 10
HEXACHLOROCYCLOPENT ADI ENE 10
2,4,6-TRICHLORO PHENOL 10
2,4,5-TRlCHLORO PHENOL 10
2-CHLORO NAPHTHALENE 10
2-NITAOANILINE 50
DIMETI IYL Pim IALA TE 10
ACENAPI Ill IYLENE 10
EHNR/DEM LABORATORY
SEMI-VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 606-20·2
u 99-09-2
u 83-32-9
u 51-28-5
u 100-02-7
u 132-64-9
u 121-14-2
u 84-66-2
u 7005-72-3
u 86-73-7
u 100-01-6
u 534-52-1
u 86-30-6
u 101-55-3
u 118-74-1
u 87-86-5
u 85-01-8
u 120-12-7
u 84-74-2
u 206-44·0
u 129-00-0
u 85-68•7
u 91-94-1
u 56-55-3
u 218-01-9
u 117-81-7
u 117-84-0
u 205-99-2
u 207-08-9
u 50-32-8
u 193-39-5
u 53-70-3
u 191-24-2
LAB NO. 6G2099
2,6-DINITROTOLUENE 10 u
3-NITROANILINE 50 u
ACENAPHTHENE 10 u
2.4-DlNlTAO PHENOL 50 u
4-NITRO PHENOL 50 u
DIBENZOFURAN 10 u
2,4-0INITROTOLUENE 10 u
DIETHYL PHTHAL.:ATE 10 ·u
4-CHLOROPHENYL PHENYL ETHER 10 u
FLUORENE 10 u
4-NITROANIUNE 50 u
4,6-DINITA0-2-METHYL PHENOL 50 u
N-NITROSODIPHENYLAMINE 10 u
4-BROMOPHENYL PHENYL ETHER 10 u
HEXACHLOROBENZENE 10 u
PENT ACHLOAO PHENOL 50 u
PHENANTHRENE 10 u
ANTHRACENE 10 u
D1-N-BUTYL PHTHALATE 10 u
FLUORANTHENE 10 u
PYRENE 10 u
BUTYLBENZYL PHTHALA TE 10 u
3,3'-DICHLOROBENZIDINE 20 u
BENZO{A)ANTHRACENE 10 u
CHRYSENE 10 u
8I5(2-ETHYLHEXYU PHTHALATE 10 u
DI-N-OCTYL PHTHALATE 10 u
BENZO(B)FLUORANTHENE 10 u
BENZO(K)FLUOAANTHENE 10 u
BENZO(A)PYRENE 10 u
INDENO( 1,2,3-CD)PYRENE 10 u
OIBENZO{A,H)ANi-HRACENE 10 u
BENZOIG,H,IIPERYLENE 10 u
DIMETHYL BENZENE
ETHYL METHYL BENZENE
ETHYL METHYL BENZENE
TRIM ETHYL BENZENE
TRIMETHYL BENZENE
TRI METHYL BENZENE
SEMIVOLATILE ORGANICS REPORT -OEM LAB PAGE 2 LAB NO. 6G2099 ------
CB.H10
C9.H12
C9.H12
C9.H12
C9.H12
C9.H12
10 T
9T
9T
_____ 1_1_T _____ TOL-Target Ouantitation Limit-Subject to
12 T change due to instrument sensitivity
9 T T-Tentatively Identified, estimated concentration
E-Estimated Value
U-Samples analyzed for this compound but not detected
N-Sample not analyzed-for this compound
0-Detected below quantitation limit
H-Holding time exceeded
COMMENTS, _______________________________________________ _
....
COUNTY
QUAD NO:
!REDELL SG OCT I::, r·:1 I: 23
REroRT TO _,01_R00""=-------Regional Office
COLLECTOR(S) : _D_A_I_I_L_EN ______ _
D,\ TE: 9n6f96
TIME
rURrOSE:
LABORATORY ANALYSIS
8OD310
COD High 340
COO LowJ35
Coliform: MF Fecal J 1616
Coliform: MF Total 31504
TOC
Turbitity
Residue., Suspended 530
T 01al Suspended solids
pll
Alkalinity to pit 4.5
Al~alinity 10 pit 8.3
Carbona1c
Bicaibonale
Carbon dio~ide
Chlo,ide
Chromium: llu 1032
Color: True 80
Cy1111ide 720
CO~IJ\IENTS:
mg/L
mg/L
mg/L
1100ml
1100ml
ms'l
NTU
mg/L
mg/L
units
mg/L
mg.IL
mg/L
mg/L
mg.IL
m!!.IL
,g/L
'"
ms'L
Owner:
Location or Site:
Descfip1ion of sampling point
Sampling Me1hod;
Remarks
Diss. Solids 70)00
Fluoride 951
Hardnes.s: 101al 900
Hardness: (non-ca,b) 902
Phenols )27)0
Specific Cond. 95
Sulfate
Sulfide 745
MBAS
Oil and Grease
Silica
Boron
NIU as N 610
TKN as N 625
Nm +N03 as n 6)0
P: Tota! Mr 665
ro,
DIVISION OF EN\'IHONl\lENTAL l\lANAGEI\IENT
Chrmislry l.11bonlory Rrporl / Gmund W•ttr Qu11lity
SAMPLE PRIORITY
~ROUTINE
~ CIIAIN OF CUSTODY
~ SAMrLF. TYPE
CIIRIS DA \'IDSON
mg/L
mg/L
mg/L
mg/L
,s'L
uMhos/cm2
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg.IL
mglL
□EMERGENCY
□
Ag-Sih·cr 46566
Al-Aluminum 46557
As-Arsenic 46551
lla-lJorium 46558
Ca-Calcium 46552
Cd-Cadium 46559
Cr-Chromium 46560
Cu-Copper 1042
Fe-Iron 1045
Ilg-Mercury 71900
K-Potassium 46555
Mg-Magnesium 927
Mn-Manganese 1055
Na-Sodium 929
Ni-Nickel
Pb-Lead 465~
Sc-Selenium
7.n_Zinc 465(,7
Lab Number 6G2I01
Date Received : 9/27196
Time Re.:ei'"ed : 9:00AM
Recei\·ed By DS
Relea~d By DS
Dale 1cported : 10/14/96
,g/L Organoch!orine Pesticides
ug/L Organophosphorus Pesticides
,g/L Nitrogen Pesticides
,g/L
mg/L Acid Herbicides
,g/L
,g/L X Semirnfotiles
,g/L TPII-Diesc1 Range
,g/L
,g/L Volatile Organics {\'QA bottle)
mg/L
ms'L TPII-Gasoline Range
ug/L TPll-lJTEX Gasoline Range
mg/L
ug/1.
ug/L
uglL
uglL
6(;2101.SEP
North Coroll110
GROUNDWATER FIELD/LAB FORM Depmlmenl of Environment, Hcallh, nnd Nolurel Rcsourcl'.?9
DIVISION OF ENVIRONMENTAL MANAGEMENT. GROUNDWATER SECTION
Counly I:,e_<!_a_ll ;l1/1Jl\J Of GLJ~TQDY
Quad No Lb--7,,_... Serial No·----~-SAMPLE PRIORIYY
Lat. 3;," 4J...' S:9 "N Long. eo"S-] 'S"Y • t..) ~ROUTINE . □EMERGENCY
~CHAIN OF CUSTODY
Report To: ARO, FRO~. RRO, WaRO, WiRO,
WSRO, Kinston FO, Fed. Trust, Cenlral 011., OIiier: ________ _
Shipped by: Bus, ~ Hand Del., Oilier· ____________ _
0
Lab Number -7'-l't'.:"'::a-t::'""~~,-T.C.,_..=---
Date Recei d .Y)
Rec'd by:_,.....,~~-From: Bu Courier Hand Del.,
Other: -------------~----
Data Entry By: ______ Ck: ______ _
Date Reported: _____________ _
~ Purpose:,..----....
Collector(s): J>s::bl .,_ Dale ...3/-2,.',_1-1 ~'i~\.~_ Time O 1 ::Jo Baselino Comp! , Compliance LUST, Pesticide Study, Federal Trust, Other: ______ _
' . (cifc1o ono)
l]ELD ANALYSES 1 7 Owner C.,h.r ·s t c·
pH,00 ~,-_, Spec.Cond.94 >:;-a~C. Localionorsile c;..., ,:!..n W::.ll 1'l
Temp.10 17 °~ _ Odor Description of sampling point -~~¥-''-il~r"_.~A,._c.r,,.,~· ,__,wr..,,_.~-kul __________________ _
Appearance c..L.."~tt"'-~4.a:: Sampling Melhod -------<=~= ·~=~ _______ Sample lnlerva1_· ______ _
~I : .1. \:-~ bailGI, elc)
Field Analysis By: y ~ Remarks l OJ n.,.., ~ ,.,,,,..,
(pumping limo, air lemp. etc.)
LABORATORY ANALYSES
BOD, 310 mg/I Diss. Solids 70300 mg/I Ag -Silver 46566 ug/1 Organochlorine Pesticides
COD High 340 mg/I Flouride 951 mq/l Al -Aluminum 46557 ugll Organophosphorus Peslicides
COD Low 335 mg/I Hardness: Total 900 mg/I As -Arsenic 46551 ug/1 Nitrogen Pesticides
Colilorm: MF Fecal 31616 1100ml Hardness (non-carb) 902 mg/I Ba -Barium 46558 ugtl
Colilorm: MF Tolal 31504 1100ml Phenols 32730 ugll Ca -Calcium 46552 mg/I Acid Herbicides --
TOG 680 mqtl Specilic Cond. 95 uMhos/cmi Cd -Cadmium 46559 Uq/1 --
Turbidity 76 NTU Sulfate 945 mall Cr -Chromium 46560 uall ?-Semivolalile Organics
Residue., Suspended 530 mgn Sulfide 745 moll Cu -Conner 46562 uqll
Fe -Iron 46563 ugtl
Hg -Mercuri 71900 ugtl Volatile Organics (VOA bottle)
pH 403 units K -Potassium 46555 mg/I --
Alkalinity lo pH 4.5 410 mgtl Mg -Magnesium 46554 mg/I TPH -Gasoline Range
Alkalinity to pH 8.3 415 mg/I Mn -Manganese 46565 ugtl TPH -BTEX Gasoline Range
Carbonate 445 mg~ NH as N 610 ma/I Na -Sodium 46556 mgll
Bicarbonate 440 mg1l --.ilili..as. l'L62' n1g1L Ni -Nickel ug/1
Carbon dioxide 405 mg/I NO + NO. as N 630 mg/I Pb -Lead 46564 ugll ~
Chloride 940 mgtl P: Total as P 665 mall Se -Selenium uqtl " Chromium: Hex 1032 Ug,'I Zn • Zinc 46567 ug/1 ......,
Color: True ao Pt-Co
Cyanide 720 mg/I
Lab Comments:--------'------------------------------------------------
GW-54 REV. 6193 For Dissolved Analysis -submit tillered sample and write "DIS" in block.
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
9B-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91 • 1
120-83·2
120-82-1
91-20-3
106-47•8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131·11·3
208-90-0
WATER
ANILINE 10
PHENOL 10
8I5(2-CHLOAOETHYL) ETHER 10
2-CHLOROPHENOL 10
1,3-DICHLOROBENZENE 10
1.4-DICHLOROBENZENE 10
BENZYL ALCOHOL 20
1,2-DICHLOROBENZENE 10
2-METHYL PHENOL 10
BIS(2-CHLOROISOPROPYL) ETHER 10
4-METHYL PHENOL 10
N-NlTAOS0-0I-N-PROPYLAMINE 10
HEXACHLOROETHANE 10
NITROBENZENE 10
ISOPHORONE 10
2-NlTRO PHENOL 10
2,4-DIMETHYL PHENOL 10
8ENZOIC ACID 50
8I5I2-CHLOROETHOXYI METHANE 10
2,4-DICHLORO PHENOL 10
1,2,4-TRICHLOAOBENZENE 10
NAPHTHALENE 10
4-CHLOROANILINE 20
HEXACHLOROBUTADIENE 10
4-CHLOR0-3-METHYL PHENOL 20
2-METHYL NAPHTHALENE 10
HEXACHLOROCYCLOPENT ADIENE 10
2,4,6-TRlCHLORO PHENOL 10
2,4,5-TRlCHLORO PHENOL 10
2-CHLORO NAPHTHALENE 10
2-NlTROANILINE 50
DIMETHYL PIITI IALA TE 10
ACENAPIITIIYLENE 10
EHNR/DEM LABORATORY
SEMI-VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS .
u 606-20-2
u 99-09-2
u 83-32-9
u 51-28-5
u 100-02-7
u 132-64-9
u 121-14-2
u 84-66-2
u 7005-72-3
u 86-73-7
u 100-01-6
u 534-52-1
u 86-30-6
u 101-55-3
u 118-74-1
u 87-86-5
u 85-01-8
u 120-12-7
u 84-74-2
u 206-44-0
u 129-00-0
u 85-68-7
u 91-94-1
u 56-55-3
u 218-01-9
u 117-81-7
u 117-84-0
u 205-99-2
u 207-08-9
u 50-32-8
u 193-39-5
u 63-70-3
u 191-24-2
2,6-0lNlTROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITRO PHENOL
4-NITRO PHENOL
DIBENZOFURAN
2.4-DINITROTOLUENE
DIETHYL PHTHALATE
4-CHLOAOPHENYL PHENYL ETHER
FLUORENE
4-NlTAOANILINE
4,6-DINITR0-2-METHYL PHENOL
N-NITROSOOIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE
PENTACHLORO PHENOL
PHENANTHRENE
ANTHRACENE
DI-N-8UTYL PHTHALATE
FLUORANTHENE
PYRENE
BUTYLBENZYLPHTHALATE
3,3'-0ICHLOROBENZIOINE
BENZO(A)ANTHRACENE
CHRYSENE
8IS12-ETHYLHEXYLJ PHTHALATE
0I-N-OCTYL PHTHALATE
BENZO(B)FLUORANTHENE
BENZO(KJFLUORANTHENE
BENZO(A)PYRENE
INOENO{l ,2,3-CD)fYRENE
DIBENZOIA,H)ANTHnACENE
8ENZOIG,H.IIPERYLENE
LAB NO. 6G2101
SUPERVISOR -'lfa~t;( ',6
DATE e,?
ENTERED BY ffi. 1
_
DATE~
10 u
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
SEMIVOLATILE ORGANICS REPORT -DEM LAB PAGE 2 LAB NO. _ __:6:..:G:..::2:..cl..:.0.:...1
NO BASE/NEUTRAL OR ACID EXTRACT ABLE ORGANICS
DETECTED BY GC/MS.
___________ TOL· Target Quantitation Limit-Subject to
change due to instrument sensitivity
T-Tentatively Identified, estimated concentration
E-Estimated Value
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound
D· Detected below quantitation limit
H-Holding time exceeded
COMMENTS: __________________________________________________ _
C -0"-1 \ · r. ':.• 1, I: 2 3 jl) I, l)
COUNTY· IREDELL
QUAD NO:
REPORT TO MRO .::_ _________ Regional Office
COLLECTOR(S) DAIi LEN
DATE: 9n6/96
TIME:
rURPOSE:
LABORATORY ANALYSIS
BODJIO
COD High )40
COD Low)J5
Coliform: MF Fecal )1616
Coliform: MF Total 31504
TDC
f urbitity
Residue., Suspended SJO
fotal Suspended solids
pl!
All.:alinity 10 ptl 4.S
Alkalinity 10 pH 8.J
Cmbonate
Bicarbonate
Carbon dio,ddc
Chloride
Chromium: Hu 1032
Colo,: True 80
Cyanide 720
COMMENTS:
mg/L
mg/L
mg/L
fl(lOml
1100ml
mg,1
NTU
mg/L
mg/L
units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
uglL
c.u.
mg/L
(h~llCf.
Location nr S11e
Dcs-c:ription ohampling point
Sampling /'.kthod:
Rc,marks·
Diss. Solids 70300
Fluoride 951
1 lardness: total 900
llardncss: (non-carb) 902 ·
rhenob )2730
Specific Cond. 95
Sulfate
Sulfide 745
MBAS
Oil and Grease
Silica
lforon
Nill as N 610
TKN as N 625
N02 +NOJ as n 6)0
P: Tola! as r 665
1'04
IJIVISION OF ENVIRONMENTAL MANAGEMENT
Chrmi.Jlry L•bor•lory Rc,iwrt /Ground W•ter Qualily
SAMPLE PRIORITY
{8JROUTrNE
~ CHAIN OF CUSTODY
~ SAMPLE TYrE
('IIHIS I),\ \'IUSON
mg/L
mg.IL
mg/L
mg/L
,g/L
uMhos/cm2
mg/L
mg/L
mg/L
mg/L
mg/L
mg.IL
mglL
mg/L
mg/L
mg/L
□EMERGENCY
□
Ag-Sil, er 46566
Al-Aluminum 46557
As-Arsenic 4655 I
Ba-£larium 46558
Ca-Calcium 46552
Cd-Cadium 46559
Cr-Chromium 46560
Cu-Copper 1042
Fe• Iron 10-15
Ilg-Mc1eury 71900
K-Potassium 46555
Mg· !llagn~sium 927
Mn-Manganese 1055
Na-Sodium 929
Ni-Nicl.:el
Pb-Lead 46564
Sc-Selenium
Zn_Zinc 465(,7
Lab Number 6G2IOO
Date Recc,i,·-,d 9127/96
Time Rec:ei,·ed 9:00AM
Rec:c,iv-,d By DS
Released By DS
Dote reportc,d : 10/14/96
,g,C Organoch!otine Pesticides
,g/L Organophosphorus Pesticides
,g/L Nitrogen Pesiicidcs
,g/L
mg/L Acid Herbicides
,g/L
og/L X Semivo!atilcs
,g/L TPII-Dicscl Range
,g/L
us)L Volatile Organics (VOA bottle)
mg/L
mg/L TPH-Gasoline Range
us)L TPII-BTEX Gasoline Range
mg/L
,g/L
og/L
us,IL
uglL
SG2100.SEP
;;;;.,
HUllll vu1u1111,..
GROUNDWATER FIELD/LAB FORM Onpartmenl of Environment, Henllt1 1 nnd Natural Rcsource9
DIVISION OF ENVIRONMENTAL MANAGEMENT -GROUNDWATER SECTION
Counly · Lrg.,d...~1-\
Quad No Lb 1 ,...., 1 Serial No. ______ _
Lal. :3S:"'i;i..' 5'9"-NLong. 8v':;·7•s'i" w ~~~P;~fJP 13 \~BrQUSTO DYO
('8ROUTINE l]EMERGENCY · ·
.,~ [8lCHAIN OF CUSTODY
Report To: ARO, FRO,~ ARO, WaRO, WiRO,
WSRO, Kinston FO, Fed. Trust, Central 011., Other: ________ _
Data Entry By: ______ Ck: ______ _
Date Reported: _____________ _
Shipped by: Bus,~. Hand Del., Other· ___________ _ Purpose:
Colleclor(s): j)cL( •·• Date q ,,l.,<. ('(I,. Time _G_'i':~-LZ~(.,~ ___ Baselinu, ~ Compliance, LUST, Pesticide Sludy, Federal Trusl, Olher: ______ _
......_ • t ~• 1c11c1o one) ·
FIELD ANALYSES 7 Owner c /,,.,;, nc:u ,..,1.,
pH400 "--£ • < Spec. Cond.94 ">S~ at ~o C Location or sile J>..-.....,;J,'.Z; We \ l =I\: :;i_
Temp. 10 / 7 °c Odor _______ Description of sampling point ~:S.!/("-'-'Jc¼:.,..,__:\'--.,,<x'-->--"<,.JU"'-"=-' ---------------------
Appearance c::,lu:-/c._,Lc,.-<-,,-f Sampling Melhod -------~=_. __________ Sample Interval _______ _
-./: ( ..J. <'J9bade1, elc)
Field Analysis By: --,J.lµ.<C;.,h=I•._~--------Remarks .-, "'-'-' .
LABORATORY ANALYSES (pemp;"glim,.,;,1omp ... ,.)
-BOD, 310 mg/I Diss. Solids 70300 mg/I Ag -Silver 4G566 ugll Organoclilorine Pesticides
COD High 340 mgt! --Flouride 951 mg/I Al -Aluminum 46557 ugll Organophosphorus Pesticides
COD low 335 mgtl Hardness: T olal 900 mg/I As -Arsenic 46551 ugll Nitroqen Pesticides
Colilorm: MF Fecal 31616 1100ml Hardness (non-carb} 902 mgtl Ba -Barium 46558 ua/I
Colilorm: MF Tola! 31504 1100ml Phenols 32730 ugll Ca -Calcium 46552 mg/I Acid Herbicides
TOG 680 mgll Specific Cond. 95 uMhos/cm2 Cd • Cadmium 46559 ugtl --
Turbidily 76 NTU Sullale 945 mgtl Cr -Chromium 46560 uqll X Semivolatile Organics
Residue., Suspended 530 rngtl Sullide 745 moll Cu -Conner 46562 uqll --
Fe -Iron 46563 ugll
Hg -Mercurr 71000 ugll Vola(ile Organics (VOA botlle)
pH 403 unils K -Potassium 46555 mg/I
Alkalinily lo pH 4.5 --410 mg/I Mg -Magnesium 46554 mgll TPH • Gasoline Range
Alkalinily to pH 8.3 415 rngll Mn -Manganese 46565 ugll TPH · BTEX Gasoline Range
Carbonale 445 mgtl NH as N GI0 mgll Na • Sodium 46556 mg/I -s --Bicarbonale 440 mg~! lKtLas.lcL.62< moil. _Ni -Nickel ugll ------
Carbon dioxide 405 mgll NO + NO as N 630 mg£!_ Pb -Lead 46564 ugll --
Chloride 940 mgll P: Tola! as P 665 mg/I Se -Selenium uqll
--Chromium: Hex 1032 ugll Zn -Zinc 46567 ug~
Color: True 80 P(-Co
Cyanide 720 mg/I
Lab Commenls: ----------------------------------------------------------
GW-54 REV. 6193 For Dissolved Analysis -submit tillered sample and wrile "DIS" in block.
__,'
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE,
62-53-3
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-,7
108-60-1
106-44-5
621·64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
WATER
ANILINE
PHENOL
815(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
BENZYL ALCOHOL
1,2-DICHLOROBENZENE
2-METHYL PHENOL
81512-CHLOROISOPROPYLI ETHER
4-METHYL PHENOL
N-NITAOSO-D1-N-PROPYLAMINE
HEXACHLOROETHANE
NlTROBENZENE
ISOPHORONE
2-NITRO PHENOL
2,4-DIMETHYL PHENOL
BENZOlC ACID
B15(2-CHLOROETHOXY) METHANE
2,4-0ICHLORO PHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOAOANILINE
HEXACHLOAOBUTADIENE
4-CHLOR0-3-METHYL PHENOL
2-METHYL NAPHTHALENE
H EXACHLOROCYCLOPENT ADIENE
2,4,6-TRICHLORO PHENOL
2,4,5-TRICHLOAO PHENOL
2-CHLORO NAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALA TE
ACENAPHTHYLENE
EHNR/DEM LABORATORY
SEMI.VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
10 u 606-20-2
10 u 99-09-2
10 u 83-32-9
10 u 51-28-5
10 u 100-02-7
10 u 132-64-9
20 u 121-14-2
10 u 84-66:2
10 u 7005-72-3
10 u 86-73-7
10 u 100-01-6
10 u 534-52-1
10 u 86-30-6
10 u 101-55-3
10 u 118-74-1
10 u ·87-86-5
10 u 85-01-8
50 u 120-12-7
10 u 84-74-2
10 u 206-44-0
10 u 129-00-0
10 u 85-68-7
20 u 91-94-1
10 u 56-55-3
20 u 218-01-9
10 u 117-81-7
10 .U 117-84-0
10 u 205-99-2
10 u 207-08-9
10 u 50-32-8
50 u 193-39-5
10 u 53-70-3
10 u 191-24-2
2,6-DINITROTOLUENE
3-NITAOANIUNE
ACENAPHTHENE
2,4-DINITRO PHENOL
4-NITRO PHENOL
DlBENZOFUAAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
4,6-DINITR0-2-METHYL PHENOL
N-NITROSODIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOAOBENZENE
PENT ACHLORO PHENOL
PHENANTHRENE
ANTHRACENE
DI-N-8UTYL PHTHALATE
FLUORANTHENE
PYRENE
BUTYLBENZYL PHTHALA TE
3,3' -DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
815(2-ETHYLHEXYLI PHTHALATE
D1-N-OCTYL PHTHALATE
BENZO{B)FLUORANTHENE
BENZO(K)FLUORANTHENE
BENZO(A)PYRENE
INDEN0(,1,2,3-CD)PYRENE
OIBENZO(A,H)AN'fHRACENE
BENZO{G,H,l)PERYLENE
LAB NO. 6G2100
SUPERVISOR~
DATE~
EN°TERED BY -'W!'=':;:::::......~-
DATE \ D\y:\:'Blt
10 u
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
SEMIVOLATILE ORGANICS REPORT -DEM LAB PAGE 2
NO BASE/NEUTRAL OR ACID EXTRACT ABLE ORGANICS
DETECTED BY GC/MS.
LAB N0. __ ;:.6G=2..:.10;:.0;:._
TOL-Target Quantitation Limit-Subject to
change due to instrument sensitivity
T-Tentatively Identified, estimated concentration
E-Estimated Value
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound
D-Detected below quantitation limit
H-Holding time exceeded
COMMENTS: _____________________ ~------------------------------
_J
•-
COUNTY
QUAD NO:
!REDELi.
FE c::: ! '-.:F ;1 .-'F
!•"· i.:: ;: ,-·1j_;: ;,_:
REPORT TO
COLLECTOR(S)
DATE:
_>_1_R_o _________ Rcgional Office
DAHLEN
11n7196
TIME:
PURPOSE·
LABORATORY ANALYSIS
800 310
COD lligh 340
COD Low ))S
Colifonn: MF Fecal 31616
Coliform: MFToto1J1504
TOC
ru,bi1i1y
Residue, Suspended SJO
foto1 Suspended solids
pll
Alh1ini1y to pll 4.S
Alkalinily lo pt! 8.)
Carbonate
llicarbonate
C.ubon dio.~ide
Chlodde
Chromium: He:,: 1032
Color: True 80 ~
Cranide 720
COMMENTS:
mg/L
mg/L
mglL
1100ml
1100ml
mg/I
NTlJ
mg/L
mg.It
units
mg/L
mg/L
mg/L
mg/L
mg/L
ms"-
,g/L ,.,
mg/L
O"Ticr·
Location or Site
Dcsc,iption of sampling point
Sampling Mc1hod:
Rcmaiks·
Diss Solids 70)00
Huo1ide 951
Hardness· 101al 900
Hardness: {non-carb) 902
rhenols J27JO
Speeific Cond. 95
Sulfate
Sulfide 7-15
MBAS
Oil and Gre,ne
Silica
Boron
NIB as N 610
n,:.N as N 625
N02 ~N03 as n 6JO
r: Total as P 665
ro,
DIVISION OF EN\'IHONI\IENTAL l\lANAGE/\IENT
Cheml,try L11bor11tory Rll'porl /Ground Waler Qu111ily
s,,r,.1r1.r~RIQRITY
□ROUTINE
~ CIIAINOFCUSTODY
0 SAMPLE TYPE
BRUCE ELMORE WEU.
mg/L
mglL
mg/L
ms"-
,g!L
u~lhoskm2
mg/L
mg/I.
mg/L
mg/L
mglL
mg/L
mg/L
mg/I.
mg/L
mg•L
(K]EMERGENCY
□
Ag-S1l,·er 46566
Al-Aluminum 46557
As-Arsenic -16551
Ba-Barium 46558
Ca-Calcium 46552
Cd-Cadium 46559
Cr-Chromium 46560
Cu-Copper 1042
Fe-Iron 10-U
1111-~lercury 71900
K-rotassium -16555
Mg-Magnesium 927
Mn-Manganese 1055
Na-Sodium 929
Ni-Nield
rb-1.ead-1656-1
Se-Selenium
Zn_Zinc -16567
Lab Number 6Gl917
Dale Received : 8/111/96
Time Received · 9:JS AM
Rccci1·cd By DS
Released By OS
Date 1cportcd : 9/4/96
,g/L O,ganochlorine Pesticides
ugl\. O,ganophosphorus resticides
,g/L Ni110gen Pesticides
,g!L
mg.IL ' Acid I lerbicides
,g/L
ugiL X Semi volatiles
,g!L TPll-Diesel Range
uglL
uBJ'L X \'ola1ile Or11anics (VOA bonle)
mg/L
mg/L l PU-Gasoline Range
,wL fPII-BTEX Gasoline Range
mg/L
ug/L
ugiL
ugil
uglL
6Gl817 AUG
GROUNDWATER FIELD/LAB FORM
County µ,-,,k if
Quad No L 1,7 w, Serial No.--~----Lat. 1<::i' '(.l' {"<;' 'Ni ong. ,C:tJ d.5-b''C'i'1 Lv
No r t 11 C: a r o 1111 o
Department of Envlronmcnl, ftcallh, nnd Natural RC?sources
DIVISION OF ENVIRONMENTAL MANAGEMENT-GROUNDWATER SECTION
Dale Reported: ______________ _ 11eporl To: ARO, FRO,~~RO, WaRO, WiRO,
WSRO, Kinston F~, Fe . Trusl, Central Off., Other:
Shipped by: Bus, our" , Hand Del., Olher· P i'\.... I. urpose· .,,.-----y Colleclor(s): ~l e,,,, llale £/2,['f'' Time 13:.:l O Baseline, CJunpl:lrnl, Compliance, LUST, Pesticide Study, Federal Trust, Olher: _______ _
/ / -"'.'""? Is ,crrcl& ono) EIELD ANALYSES ;.. 1. Owner /'id,,, l=,/.,,-,~µ"--~-----------------
p1-t,00 ,.,_£:CJ_ Spec.Cond.94 i/tl at-,>5°C Localionorsite /<) Le:;~, '7> -S{<(c?:J'-',il, ,Jc5'1,·Tl
Temp.
10
: b 0 c Odor 5f,,:,,.,,,: Description of sampling poinl ~~:-R='J<d;,"-'-'-. _.c~~~__,,l:,"-,c:,.__._<+l''--~7,._a,..,;"""'.-<'-"f..~---------------
Appearance cJ,:":cl,~ => Sampling Method @ Sample Interval _______ _ 1~a1tar,olc)
Field Analysis By:l, /¢.,,,. Remarks-----------=-~-~~~~~---------------(pumpino time. air tamp. e1c )
LABORATORY ANALYSES
BOD. 310 n~~ Diss. Solids 70300 rngtl Ag -Silver 46566 ·ugtl O,ganochlodne Pesticides
------
COD High 340 mg/I --Flouride 951 mg1 /\I -Aluminum 46557 ug!f Organophosphorus Pesticides
COO Low 335 miJI! --Hardness: Total 900 n1u!l. As -A, scnic 46551 ugtl Nilro9en Peslicides
Coliform: MF Fecal 31616 II 00ml Hardness {non-carb} 902 mq/1 Oa -Barium 46558 ug/I .
Coliform: MF T olal 31504 1100ml Phenols 32730 uall Ca -Calcium 46552 mg/I ;>< Acid Herbicides
·-
TOC 660 mg/I ._Sgecific Cond. 95 uMhos/cm1 Cd -Cadmium 46559 ug/I --
Turbidity 76 NTU Sulfale 945 mg!!_ Cr -Chromium 46560 ugll L-,X,_ Sernivolatile Organics
--
Residue., Suspended 530 111g{I Sullide 745 mil{!_ --Cu · Coeeer 46562 ugll ------Fe -Iron 46563 ug/1 ' H~ -Mercurl 71900 ugll >< Volalile Organics (VOA bollle)
--pH 403-units K -Potassium 46555 mg/I ----Alkalinity to pH 4.5 410 mg/I Mg • Magnesium 46554 mq/l TPH -Gasoline Range
--Alkalinily lo pl I 0.3 415 111911 Mn -Manoancse 4G5G5 uq/I TPH -BTEX Gasoline nango --Carbonate 445 mg/I NH. as N G10 mg~L Na -Sodium 46556 mgtl tj ------
--Bicarbonate 440 mg/I --JJfrLas..tLJi2< -g1l --Ni -Nickel ug/I ~ ~ Carbon dioxide 405 mgll NO + NO, as N 630 mgfl_ Pb -Lead 46564 ug/1
Chloride 940 mg/I P: Total as P 665 mq/1 Se • Selenium ug/1 )
--
Chromium: Hex 1032 ugll Zn -Zinc 46567 UQ/1
Color: True BO Pt-Co
Cyanide 720 mgtl
Lab C01nrnenls: -----------------------------------------------------------
GW-54 REV. &'93 For Dissolved Analysis -submit lilteied sample and wrile "DIS" in block.
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
75.35-4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79-34-5
TQL-
T-
E-
U-
N-
0-
M-
COMMENTS:
WATER
1, 1-Dichloroethene 0.75
Methylene Chloride 10
lrans-1,2-Dichloroelhene 0.75
1, 1-Dichtoroethane 0.25
2,2-Dichloropropane 0.25
cis-1.2-Dichloroethene 0.25
Chloroform 0.25
Bromochloromethane 0.75
1, 1, 1-Trichloroethane 0.25
1, 1-Dichloropropene 0.25
Carbon Tetrachloride 0.75
1,2-Dichloroethane 0.25
Trichloroethene 0.25
1,2-Dichloropropane 0.25
Bromodichloromelhane 0.25
Dibromomelhane 1
cis-1, 3-Dichloropropene 0.25
trans-1, 3-Dichloropropene 0.25
1, 1,2-Trichloroethane 0.25
Tetrachloroethene 0.25
1.3-Dichloropropane 0.25
Dibromochloromethane 0.75
1,2-Dibromoethane 1
Chlorobenzene 0.25
1, 1, 1,2-Telrachloroelhane 0.25
Bromoform 0.5
1, 1,2,2-Telrachloroethane 0.75
Targel Quanlila!ion limit-Subject to
change due to instrument sensitivity
Tentatively Identified, not confirmed
Estimated Value
Samples analyzed for this compound but not detected
Sample not analyzed for this compound
Detected below quantilalion limit
GC/MS Analysis performed
EHNR/OEM LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 96-18-4 1,2,3-Trichloropropane
u 108-86-1 Bromobenzene
u 95-49-8 2-Chlorololuene
u 106-43-4 4-Chlorotoluene
u 541-73-1 1,3-Dichlorobenzene
u 106-46-7 1,4-Dichlorobenzene
0.39 95-50-1 1,2-Dichlorobenzene
u 96-12-8 1,2-Dibromo-3-Chloropropane
u 120-82-1 1,2,4-Trichlorobenzene
u 87-68-3 Hexachlorobutadiene
u 87-61-6 1,2,3-Trichlorobenzene
0.65 1634-04-4 Melhyl-lert-butyl ether
u 71-43-2 Benzene
u 108-88-3 Toluene
u 100-41-4 Ethyl benzene
u 108-38-3 m,p-Xylenes
u 95-47-6 a-Xylene
u 100-42-5 Styrene
u 98-82-8 lsopropylbenzene
u 103-65-1 n-Propylbenzene
u 108-67-8 1,3,5-Trimelhylbenzene
u 98-06-6 tert-Butylbenzene
u 95-63-6 1,2,4-Trimethylbenzene
u 135-98-8 sec-Butylbenzene
u 99-87-6 p-isopropyltoluene
u 104-51-8 n-Butylbenzene
u 91-20-3 Naphlhalene
Gasoline Range Estimated Total Petroleum Hydrocarbon
Other purgeables detected
(up to 1 O highest peaks)
SEVERAL UNIDENTIFIED PEAKS OETEECTED BY GCIPID.
LAB NO. 6G1917
0.25 u
1 u
0.25 u
0.25 u
0.25 u
0.25 u
0.25 u
u
0.25 u
0.25 u
0.75 u
5 u
1 u
4.9
1.2 E
2 5.8 E
1 u
2 21
u
1.3
13E
u
2 21
u
.1 u
2 6.5
2.1
mg/l mgfl
0.25 N
Detected
ugfl
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
62-53-3
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621•64·7
67-72-1
99.95.3
78-59-1
88-75-5
105-67·9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-4 7-8
87-68-3
59-50-7
91-57-6
77.47.4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
WATER
ANILINE 10
PHENOL 10
B1S12-CHLOROETHYU ETHER 10
2-CHLOROPHENOL 10
1,3-DICHLOAOBENZENE 10
1,4-DlCHLOROBENZENE 10
BENZYL ALCOHOL 20
1,2-DICHLOROBENZENE 10
2-METHYL PHENOL 10
B1S(2-CHLOAOISOPROPYL) ETHER 10
4-METHYL PHENOL 10
N-NITROSO-D1-N•PAOPYLAMINE 10
HEXACHLOROETHANE 10
NITROBENZENE 10
ISOPHORONE 10
2-NITAO PHENOL 10
2,4-DlMETHYL PHENOL 10
BENZOIC AClD 50
BISl2-CHLOROETHOXY) METHANE 10
2,4-DICHLOAO PHENOL 10
1,2,4-TRICHLOROBENZENE 10
NAPHTHALENE 10
4-CHLOROANILINE 20
HEXACHLOROBUT ADIENE 10
4-CHLOR0-3-METHYL PHENOL 20
2-METHYL NAPHTlfALENE 10
HEXACHLOROCYCLOPENT ADIENE 10
2,4,6-TRICHLORO PHENOL 10
2,4,5-TRICHLOAO PHENOL 10
2-CHLORO NAPHTHALENE 10
2-NlTROANILINE 50
DIMETHYL PHTHALATE 10
ACENAPHTHYLENE 10
EHNR/DEM LABORATORY
SEMI-VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 606-20-2
u 99-09-2
u 83-32-9
u 51-28-5
u 100-02-7
u 132-64-9
u 121-14-2
u 84-66-2
u 7005-72-3
u 86-73-7
u 100-01-6
u 534-52-1
u 86-30-6
u 101-55-3
u 118-74-1
u 87·86-5
u 85-01-8
u 120-12-7
u 84•74-2
u 206-44·0
u 129-00-0
18 85-68-7
u 91-94-1
u 56-55-3
u 218-01-9
17 117-81-7
u 117-84-0
u 205-99-2
u 207-08-9
u 50-32-B
u 193-39-5
u 53-70-3
u 191-24-2
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITRO PHENOL
4-NITRO PHENOL
DIBENZOFURAN
2,4-DINITAOTOLUENE
DIETHYL PHTHALATE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
4,6•D1NITA0·2·METHYL PHENOL
N-NITROSODIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE
PENTACHLORO PHENOL
PHENANTHRENE
ANTHRACENE
DI-N-BUTYL PHTHALATE
FLUORANTHENE
PYRENE
BUTYLBENZYL PHTHALA TE
3,3'-DICHLOROBENZIDlNE
BENZO(A)ANTHRACENE
CHAYSENE
8ISf2-ETHYLIIEXYU PftTHALATE
OI-N-OCTYL PHTHALATE
BENZOIBJFLUORANTHENE
BENZO(K)FLUORANTHENE
BENZO(A)PYRENE
INDENO(l ,2,3-CD)PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO!G,H,l)PERYLENE
LAB NO. 6G1917
SUPERVISOR~
DATE~
ENTERED BY~ 1
DATE~
10 u
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
'
SEMIVOLATILE ORGANICS REPORT -DEM LAB PAGE 2
DIMETHYL BENZENE CB.HlO 180 T
ETHYL METHYL BENZENE C9.H12 130 T
ETHYL METHYL BENZENE C9.H12 59 T
ETHYL METHYL BENZENE C9.H12 110 T
TRIMETHYL BENZENE C9.H12 96 T
TRIMETHYL BENZENE C9.H12 180 T
TRlMETHYL BENZENE C9.H12 95 T
ETHENYL METHYL BENZENE C9.H10 52 T
DIETHYL BENZENE C10.H14 43 T
DIETHYL BENZENE C10.H14 57 T
METHYL PROPYL BENZENE C10.H14 21 T
ETHYL DIMETHYL BENZENE C10.H14 22 T
ETHYL DIMETHYL BENZENE C10.H14 26 T
TETRAMETHYL BENZENE C10.H14 20 T
TETAAMETHYL BENZENE C10.H14 24 T
METHYL PROPENYL BENZENE C10.H12 31 T
METHYL NAPHTHALENE C11.H10 15 T
DIMETHYL BENZOIC ACID C9.H10.02 24 T
UNIDENTIFIED 28 E
UNIDENTIFIED 15 E
GASOLINE DETECTED BY GC/MS.
LAB NO. __ ..::6..::G..::1.::.9..::1 -'-7
TOL· Target Ouantitation limit• Subject to
change due to instrument sensitivity
T-Tentatively Identified, estimated concentration
E-Estimated Value
U-Samples analyzed for this compoufld but not detected
N-Sample not analyz~d for this compound
0-Detected below quantitation limit
H-Holding time exceeded
COMMENTS, ________________________________________________ _
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
15972-60-8
309-00-2
1912-24-9
319-84-6
319-85-7
319-86-8
58-89-9
57-74-9
5103-71-9
5103-74-2
3734-48.J
2675-77-6
501-15-6
2911-88-2
1897-45-6
1861-32-1
53-19-0
72-54-8
3424-82-6
72-55-9
789-02-6
50-29-3
60-57-1
959-98-9
33213-65-9
1031-07-8
50594-66-6
25057-89-0
133-90-4
94-75-7
94-82-6
1918-00-Q
51-36•\._.,'
KAK 'l(fl/t.,
VA VA-
CY Cl/-
WATER
ALACIILOR
ALDRIN
ATRAZINE
BHC-ALPHA
BIIC-BETA
BHC-DELTA
BHC-GAMMA(LINDANEl
CIILORDANE, TECIINICAL
CHLORDANE-ALPHA
CHLORDANE-GAMMA
CHLORDENE
CIII.ORNEB
CHLOROBENZILATE
CHLORPYRJFOS
CIILOROTIIALONIL
DCPA
DOD. OP
DOD, PP
ODE. OP
ODE. PP
DDT. 01'
DDT. PP
DIELDRIN
ENDOSULFAN I
ENDOSULFAN II
ENDOSULFAN SULFATE
ACIFLUORFEN (BLAZER)
BENTAZON
CIILORAMBEN
2.4-D
2.4-08
DCPA (ACID METABOLITES)
OICAMBA
3,5 OICIILOROBENZOJC ACID
EHNR/DEM LABDRA TORY PESTICIDES ANALYTICAL REPORT
ANALYSIS RESULTS
0.IO N 72-20-8 ENDRIN
0.08 N 7421-93-4 ENDRIN ANDEIIYDE
0.75 N 53494-10-5 ENDRIN KETONE
n.02 N 2593-15-9 ETHAZOLE
0.03 N 76-44-R IIEPTACIILOR
0.03 N l024-57-J IIEPTACIILOR EPOXIDF.
ll.01 N 118-74-1 I IEXACllLOROBENZENE
O.Jtl N 121-75-5 ~IAL,\TIIION
0.02 N 72-43-5 METIIOXYCHLOR, PP
0.03 N 2385-85-5 MIREX
0.02 N 39765-80-5 TRANS-NONACIILOR
0.03 N 26880-48-8 OXYCIILORDANE
5.00 N 52645-53-1 MIXED-PERMETflRIN
fl.OR N 1918-16-7 PROPACI/LOR
0.03 N 117-18-0 TECNAZENE
0.02 N 1582-09-8 TRIFLURALIN
0.06 N 12674-11-2 AROC!ILOR 1016
0.04 N 11104-28-2 AROCIILOR 1221
0.05 N 1114\-16-5 AROCIILOR 1232
0.02 N 5)469-21-9 AROCIILOR 1242
11.04 N 11671-19-6 AROCIILOR 1148
0.06 N 11097-69-1 AROCIILOR 1254
0.02 N I !096-82-5 AROCIILOR 1260
0.03 N 37324-23-5 AROCIILOR 1262
0.01 N 8001-35-2 TOXAPIIENE
0.02 N UNIDENTIFIED PEAKS DETECTED
ACID HERBICIDES BY ELECTRON CAPTURE DETECTION
0.50 u 120-36-5 DICIILORPROP.
5.00 u 88-85-7 DINOSEB
0.50 u 7(,IXJ-50-2 5-IIYDROXYOICAMOA
1.60 u 11Xl·02-7 4-NITROPIIENOL
5.00 u 87-86-5 PENTACIILOROPIIENOL (PCP)
0.36 u 1918-02-1 PICLORAM
0.35 u 93-76-5 2,4,5-T
0.50 u 93-72-1 2,4.5-TP (SIL VEX)
llNIOENTlr-lED rEA KS DETECTED
LAB NO.
SUPERVISOR
DATE
ENTERED BY
DATE
0.03
0.05
0.04
0.03
0.02
0.01
0.01
0.08
0.05
0.03
0.02
0.02
1.00
0.10
0.02
0.03
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
1.50
8.50
0.40
2.00
4.00
0.30
1.00
0.75
1.50 -~
6G1917
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
u
u
u
u
u
u
u
I u
1
•
786-19-6
2921-88-2
50-29-3
298-03-3
JJJ-41-5
62-73-7
60-51-5
298-04-4
2497-06-5
2497-07-6
2 !04-64-5
56)-12-2
13194-48-4
15972-60-8
834-12-8
I 912-24-9
314-40-9
23 I 84-66-9
2008-41-5
5234-611-5
101-21-3
1134-23-2
2921-88-2
333--41-5
951-51-1
759-94-4
22224-92-6
51235-04-2
51218-45-2
LAB#
PESTICIDES REPORT -DEM LAB PAGE 2
ORGANOPHOSPHATE PESTICIDES BY FLAME PHOTOMETRIC DETECTION
CARBOPIIENOTIIION
CIILORPYRIFOS
DEF
DEM ETON
DIAZINON
OICIILORVOS
DIMETHOATE
DISULFOTON
DISULFOTON SULFONE
DISULFOTON SULFOXIDE
EPN
ETIIION
ETHOPROP
ALACIILOR
AMETRYN
ATRAZINE
BROMACIL
BUTACIILOR
BUTYi.ATE
CARBUXIN
CIILORPROPIIAM
CYCLOATE
CIILORPYRIFOS
DIAZINON
OIPIIENAMID
EPTC (EPTAM)
FENAMIPIIOS
HEXAZINONE
METOLACIILOR
TOL-Target Ouantitation Limit-Subject to
change due to instrument sensitivity
T-Tentatively Identified. not confirmed
E-Estima1ed Value
NIT
1.0 N
I.I N
2.5 N.
2.5 N
0.8 N
2.1 N
3.5 N
1.0 N
2.3 N
NE N
4.0 N
1.J N
2.0 N
,
0 EN P
3.4 N
I.I N
0.8 N
3.4 N
4.8 N
2.2 N
<i.5 N
4.2 N
2.4 N
1.0 N
0.5 N
2.8 N
2.3 N
1.2 N
5.1 N
4.2 N
55-38-9 FENTIIION 2.0
115-90-2 FENSULFOTIIION 10.0
150-50-5 FOLEX 2.0
6923-22"4 MEVINPHOS 1.9
JOO-76-5 MONOCROTOPIIOS 10.0
56-38-2 NALED 4.0
298-00-0 ETIIYL PARATIIION 0.7
298-02-2 METIIYL PARATIIION 1.5
299-84-3 PIIORATE 1.5
3689-24-5 RONNEL 0.8
13071-74-9 SULFOTEPP 0.3
7786-34-7 HRBUFOS I.I
UNIDENTIFIED PEAKS DETECTED
PD
2l087-64-9 METRIBUZIN 1.6
113-48-4 MGK264 5.1
2212-67-1 MOLIN ATE 2.1
15299-99-7 NAPROPAMIDE 2.6
27314-13-2 NORFLURAZON 7.1
1114-71-2 PEBULATE 6.7
1610-IX-U PROMETUN 1.5
7287-19-6 PROMETRYN 2.4
2]950-58-5 PRON AMIDE 7.6
139-40-2 PROPAZINE 1.0
122-34-9 SIMAZINE I.I
1014-70-6 SIMETRYN 2.2
34014-18-1 TEBUTIIIURON 3.1
5902-51-2 TERBACIL 4.4
886-50-0 TERBUTRYN 1.4
1929-77-7 VERNOLA TE 0.6
UNIDENTIFIED PEAKS DETECTED
N-Sample not analyzed for this compound
0-Detected below quantitation limit
NE-No established TQL
U-Samples analyzed for this compound but not detected
6G1917
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
COMMENTS: ----------------------------------------------------------
------------------------------~,------
r
COUNTY
QUAD NO
IREDEl,L
Pi:~ci.: ! VF. U/ F:: ~~i~ c. :~:: _ C;,: ,1_::: ;,1 ·1·:_,.·.1 1. 1; ::; EC. u1v1s10N 01.-ENvmoNMENTAL l\lANAGEl\ltNT
Chemi1try L111Jon1lor)· ReJIOrl I Ground W11tn Q1111lil)'
p :·i ?. , 0 3 SAMPLE PRIQRll Y
[8JROUTINE □EMERGENCY
REPORT TO
COLLECTOR{S} :
o'o'c"aOc.._ ________ Rcgional OOicc □ CHAIN OF CUS J"ODY
EJ SAMPLE TYPE
l>AIILEN
D,\ rE:
llME:
l'URPOSE:
816/96 .
LAIJORATORY ANALYSIS
BOD JI0
COD lligh 340
COO Low JJ5
Coliform: MF Fecal 31616
Coliform: MF Tota.I J 150.1
roe
furbitity
Residue , Suspc,nd~ SJO
fatal Suspended solids
pll
Alkalinity 10 pl I 4. S
,\lka!inity to pll !IJ
Carbonate
Bicatbonate
Carbon dio~ide
Chloride
Chcomium lk~ 1032
Color: True 110
C) Mide no
CU,\IMf.NTS:
mg.IL
rng/L
mJ!/L
1100ml
/IOOrnl
mwl
NfU
llli.,'L
mg!l.
un1Ls
mg'L
mglL
m[l/L
mg/L
mg.'L
mg'L
ug.11.
'"
m!l'L
l.oca1io11 or Si1c.
Oc?>Criplion of sampling poin1
Sampling Method
Rcma,~s
()ju Solids 70300
Fluo1idc 95 I
llardncu-101a! 900
I lardness: (non-carb) 902
l'hcno1s J27JO
Specific Cond. 95
Sulfate
Sulfide 745
MLIAS
Oil and GrcJ.Sc
Silica
Boron
NIIJ as N 610
l KN as N 625
N02 +NOJ as n 630
r. lo1alasr665
1'04
{"IIRISU,\\'lllSON
ms'L Ag-Sih er 46S66
mg/L Al-Aluminum 46557
mg/L As-Arsenic 46551
mg.IL Ba-Barium 465511
""' Ca-Calcium 46552
uMhoYcm2 Cd-Cadium 46559
mg.IL Cr-Chromium 46560
mg,L Cu• Copper 1041
mg.IL Fe· Iron 10-H
ms'L Ilg-Mercury 71900
mg1L K-Po1as~ium 46555
'-lg· '-lagnesium 927
Mn-'-la,,gm,esc 1055
mg.IL Na· Sodium 929
m[l/L Ni-Nickel
n,g.lL l'b-Lcad 4t'.>S64
111g11. Sc-Selenium
mgll, 7.n 7.mc 465t,7
l,ab Numl>(r (,{;1724
Date Rccci>td 8/7{'16
Time Rccci,cd 12 ~5 PM
Rccci,cd fl) JG
Rc!c11.1cd By DS
D,lc ,cpo,tcd · %08)0
"g/1. X Orga,uxhlorinc rn1icidcs
ug/L X U1ganophosphoru1 rcs1icidcs
ug/L Niuogcn Pnlicidcs
"""' mg.IL Acid Jlc,bicidc'I
"'" "g/1. Scmi,ola11lc'I
"g/1. I Pll-Uicsd Range
""' "•' X Vola1i!c u,~anics (VOA bonk)
mg;L
m"'L rrll-Gawlinc Range
ug.lL I Pll-8 TEX Gnolinc Range
mgiL
"g/L
U!_tlL
ug•L
ugil.
IIG\124 AUO
GROUNDWATER FIELD/LAB FORM
County ;;;rd{! l'-~lf\li'.l n~ r.us100
QuadNo Lc,7,-,, 1 SerialNO.----~-•-•f~Mliu~•\:Jmdf:iii-v
Lat. 35°~ $'.L'j f•)J Long. 8Cf'J..,7' :,-,,-,
[2'.IRO"E}E □EMERGENCY
CHAIN OF CUSTODY
V
Report To: ARO, FRO~d.1rno, WaRO, WiRO,
WSRO, Kinston FO, Fed. Trust, Central OIi .. Other: ________ _
Norlh Corollno
Department of Environment, Health, end Natural Resources
DIVISION OF ENVIRONMENTAL MANAGEMENT-GROUNDWATER SECTION
ourier, H d Del., 0
Lab Number --:::'-f<'!'--f-'e7-'-""'---'---,--:;-::-:-:-,,---
Date Received ~.£..,,L..:=:::._-;<?
Rec'd by:..,,_...,.,,;z.,,__ From: Bus
Other: _______________ _
Data Entry By: ______ Ck: ______ _
Date Reported: _____________ _
Shipped by: Bus,c~and Del., Other· ___________ _
· · '-f.. { .,:;i// /c:,1 ·-. -Purpose: ~1 Collector(s): /hi -4 Date '=(">L'"< b Time /5 -15 Baseline,,(;Kmpla (,Compliance*LUST, Peslicide Sludy, Federal Trusl, Olher: '-•cl• ono) FIELD ANALYSES 7.:;, 0 Owner Ct,,:;<, U o .. l ·.: \,-'<ii ).,
atW C Location or site ----------,---,------------------------
Description ol sampling point _ _;h.:c..,"c.,'"'---'{,2.L"'--------------------------
Sampling Method _______ _,,/::::Jc.,,<-"f-_ .. c.t.;~,.~,1c~I--------Sample Interval _______ _
Remarks-----------~---===-=,--,,------------------(pumping time, ■ir 1■"'1). tic.}
pH,00 ~ '--• 0 Spec. Cond.94 ~
Temp:
10
~' 0 c Odor ______ _
Appearance_ c(a,; a_<"" (~G, cc
Freid Analysis By: _,&_,,,__ ... ,(_,,,(...:=,_=---------
LABORATORY ANALYSES
BOD 310 mQ/1 Diss. Solids 70300 mg!I Aa -Silver 46566 ua/1 ~ Organochlorine Peslicides
COD High 340 mg/I Flouride 951 mrul Al -Aluminum 46557 ua/1 Organophosphorus Pesticides
COD Low 335 · mg/I Hardness· Total gno mall As -Arsenic 46551 unn Nilroaen Pesticides
Colilorm: MF Fecal 31616 1100ml Hardness tnon-carb\ 902 mail Ba -Barium 46558 UQ/1
Colilorm: MF Total 31504 1100ml Phenols 3?730 un" Ca -Calcium 46552 mo/I Acid Herbicides
TOG 680 mQII Soecilic Cond. 95 uMhos/cm2 Cd -Cadmium 46559 ua/1
Turbidity 76 NTU Sullate 945 mail Cr -Chromium 46560 uQ/1 Semivolatile Organics
Residue., Suspended 530 mg/I Sullide 745 mail Cu -Conner 46562 uQII
Fe • Iron 46563 uo/1 .
Ho• Mercurv 71900 uo/1 I':>< Volalile Organics (VOA bo1tle)
pH 403 unit~ K -Potassium 46555 mgl
Alkalinity to pH 4.5 410 mg/I Mq -Maonesium 46554 mc,1 TPH • Gasoline Range
Alkalinity lo pH 8.3 415 mg/I Mn -Manoanese 46565 ua/1 TPH · BTEX Gasoline Range
Carbonale 445 mg/I NH. -as N 610 mClil Na • Sodium 46556 mQII
BicorbOnate 4-40 mail I~~ as~ 625 mgll Ni· t,/i~~el lill-'l / ...... /
Carbon dioxide 405 mQ/1 NO +NO as N 630 mrul Pb -Lead 46564 ua/1 J /
Chloride 940 mg/I P: Total as P 665 ma1I Se -Selenium unn . I/ /
Chromium: Hex 1032 ug1I Zn -Zinc 46567 unn
Color: True eo P1-Co
Cyanide 720 mg/I
Lab Comments:------------------------------------------------------
GW-54 REV. 6193 For Dissolved Analysis -submit filtered sample and write "DIS" in block.
.REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
15972-60-8
309-00-2
1912-24-9
319-84-6
319-85-7
319-86-8
58-89-9
57.74.9
5103-71-9
5103-74-2
3734-48-3
2675-77-6
501-15-6
2921-88-2
1897-45-6
1861-32-1
53-19-0
72-54-8
3424-82-6
72-55-9
789-02-6
50-29-3
60-57-1
959-98-9
33213-65-9
1031-07-8
50594-66-6
25057-89-0
133-90-4
94-75-7
94-82-6
1918-00-9
51-36-5
WATER
ALAC!lLOR
ALDRIN
ATRAZINE
B!IC-ALPIIA
BHC-BETA
BHC-DELTA
BllC-GAMMAtUNDANE)
CHLORDANE, TECHNICAL
CIILORDANE-ALPIIA
CIILORDANE-GAMMA
CIILORDENE
CIILOR:NEB
CIILOROBENZILATE
Cl/1.0RPYRlr=oS
CIILOROTIIALONIL
DCl'A
ODD.OP
DOD, PP
ODE, OP
DOE. PP
oor. OP
DDT. PP
DIELDRIN
ENDOSULFAN I
ENDOSULFAN 11
ENDOSULFAN SULFATE
ACIFLUORFEN (BLAZER)
BENTAZON
CHLORAMBEN
2.4-D
2.4-D8
DCPA (ACID METABOLITES)
DICAMBA
3.5 DICIILOROBENZOIC ACID
EHNR/DEM LABO RA TORY PESTICIDES ANALYTICAL REPORT
ANALYSIS RESULTS
0.IO u 72-20-8 ENDRIN
0.08 u 7421-93-4 ENDRIN ANDEIIYDE
0.75 u 53494-70-5 ENDRIN KETONE
0.02 u 2593-15-9 ETIIAZOLE
O.OJ u 76-44-8 IIEPTACHLOR
0.03 u 1014-57-3 IIEPTACHLOR EPOXIDE
(l.()I u 118-74-1 1 IEXACIILOROBENZENE
O.JU u I 21-75-5 M,\LATIIJON
0.02 u 72-43-5 METHOXYCIILOR. PP
0.03 u 2385-85-5_ MIREX
0.02 \J 39765-Ro-'s TRANS-NONACIILOR
0.03 \J 2688.0-411-8 OXYCIILORDANE
.. 5.00 u 52645-53-1 MIXEO-PERME"J IIRIN
(I.OR II 19111-1<1-7 l'ROPACIILOR
0.03 u 117-18-0 ·1 ECNAZENE
0.02 \I 1582-09-8 TRIFLURALJN
0.06 u 12674-11-2 AROCHLOR !016
0.04 u I I I04-28·2 AROCIILOR 1221
0.05 u 11141-16-5 AROCIILOR 1232
0.02 II 534(19-21-9 AROCIILOR 1242
u.o.t \I I 2<,7 2-29-h ,\ROCHLUR 11411
0.06 u 11097-69-1 AROCHLOR 1254
0.02 u 11096-82-5 AROC!lLOR 1260
0.03 u 37324-23-5 AROCIILOR 1262
0.01 u SlXJl-35-2 TOXAPllENE
0.02 u UNIIJEN"l'IFIEI> PEAKS 1Jt.:n:cn:1,
0.50 N 120-36-5 DICHLORPROP
5.00 N 88-85-7 DINOS EB
0.50 N 7600-50-2 5-HYDROXYDICAMBA
1.60 N 100-02-7 4-NITROP/IENOL
5.00 N 87-86-5 PENT ACIILOROPIIENOL {PCP)
0.36 N 1918-02-1 PICLORAM
0.35 N 93-76-5 2,4,5-T
0.50 N 9)-72-1 2,4,5-TP (SILVEXJ
UNIDENTIFIED PEAKS DETECTED
LAB NO. 6G1724
SUPERVISOR~· .. _ DATE :,.
\
ENlERED BY
DA 1 E _ /27_j'31a
O.oJ u
0.05 u
0.04 u
0.03 u
0.01 u
0.01 u
{1.01 II
O.!JH u
0.05 u
0.03 u
0.02 u
0.02 u
1.1:KJ u
ll.10 u
O.o2 u
(J.(J) \I
o.5n \I
U.50 \I
0.50 \I
0.50 II
0.50 \I
0.50 u
0.50 u
0.50 u
1.50 u
2
8.50 N
0.40 N
2.00 N
4.00 N
0.30 N
1.00 N
0.75 N
I.SO N
•
786-19-6
2921-88-2
50-29-J
298-03-3
333-41-5
62-73-7
60-51-5
298-04-4
2497-06-5
2497-07-6
2104-64-5
563-12-2
131 94-48-4
15972-60-8
834-12-8
1912-24-9
314-40-9
23184-66-9
2008-41-5
5234-68-5
101-21-3
1134-23·2
2921-88-2
333-41-5
957-51-7
759-94-4
22224-92-6
51235-04-2
51218-45-l
CARBOl'IIENOTIIION
CHLORPYRIFOS
DEF
DEM ETON
OIAZINON
DICJILORVOS
DIMETIIOATE
DISULfOTON
DISULFOTON SULFONE
DISULFOrDN SULFOXIDE
EPN
ETIIION
ETHOPROP
ALACIILOR
AMETRYN
ATRAZINE
0ROMACIL
BUTACllLOR
BUTYLATE
CARBOXIN
CIILORPROPIIAM
CYCLOATE
CIILORPYRIFOS
OIAZINON
OIPIIENAMIO
EPTC {EPTAM)
FENAMIP\10S
IIEXAZINONE
METOLACHLOR
TGL-Target Ouantitation Limit-Subject to
change due to instrument sensitivity
T· Tentatively Identified, not confirmed
E-Estimated Value
PESTICIDES REPORT -DEM LAB PAGE 2
1.0 u 55-38-9
1.1 u 115-90-2
2.5 u 150-50-5
2.5 u 6923-22-4
0.8 u 300-76-5
2.1 u 56-38-2
).5 u 29R-aJ.o
1.0 u 298-02-2
2.J u 299-84-]
NE u 3689-24-5
4.0 u 13071-74-9
. I .J u 771Ui-34-7
2.0 u
NITROGEN PESTICIDES BY NP DETECTION
).4 N 21087-64-9
I.I N 113-48-4
0.8 N 2212-67-1
).4 N t 52Q9.Q9-7
4.8 N 27314-13-2
2.2 N 1114-71-2
,,.5 N lhlO•l/Hl
4.2 N 7187-19·6
2.4 N 23950-58-5
1.0 N I 39-40-2
0.5 N 122-]4-Q
2.8 N tnl4-70•6
2.J N 34014-18-1
1.2 N 5902-51-2
5.7 N IIHfl-50-11
4.2 N 1919-77-7
N-
0-
NE-
U-
LAB ll 6G 1724
FENTIIION 2.0 u
FENSULFOTIIION 10.0 u
FOLEX 2.0 u
MEYINPIIOS 1.9 u
MONOCRO"IOPI\OS 10.0 u
NALED 4.0 u
ETIIYL PARAllllON 0.7 u
METIIYL PARATIIION u u
PIIORATE 1.5 u
RONNEL 0.8 u
SULFOTEl'I' 0.J u
TERBUFOS I. I u
UNIDENTIFIED PEAKS DETECTED 0
METRIBUZIN 1.6 N
MGK264 5.1 N
MOLIN ATE 2.1 N
NAPROPAMJOE 2.6 N
NORfLURAZON 7.1 N
PERU LATE 6.7 N
l'IWME'JUN l.:i N
PROMETRYN 2.4 N
PRON AMIDE 7.6 N
PROPAZINE 1.0 N
SIMAZINE I.I N
SIMETRYN 2.2 N
TEBUTIIIURON J. I N
TERBACIL 4.4 N
TERHUlRYN 1.4 N
VERNOLA TE 0.6 N
UNDIENTIFIED PEAKS DETECTED
Sample not analyzed for this compound
Detected below quantitation limit
No established TQL
Samples analyzed for this compound but not detected
COMMENTS:-----------------------------------------------
•
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
75-35·4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-87-5
. 75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79-34-5
TQL-
T-
E
U-
N-
D-
M·
COMMENTS:
BWC SJ.(,
~?C,
WATER
1, 1-Dichloroe~hene
Methylene Chloride
trans-1,2-Dichloroethene
1, 1-Dichloroethane
2. 2-Dichloropropane
cis-1.2-Dichloroethene
Chloroform
Bromoch!orome1hane
1, 1, 1-Trichloroethane
1, 1-Dichloropropene
Caibon Tetrachloride
1.2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Br ornod ichl or o methane
Oibrornometl1ane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1, 1,2-Trichtoroethane
Telrachloroelhene
1,3-Dichloropropane
Di bro mo chi or ome thane
1,2-Dibromoethane
Chlorobenzene
1, 1, 1,2-Tetrachloroethane
Bromororm
1, 1,2,2-Tetrachloroethane
Targel Ouantitation limil-Subject to
change due to instrument sensitivity
Tentatively Identified. not conlirrned
Es1imated Value
0.75
10
0.75
0.25
0.25
0.25
0.25
0.75
0.25
0.25
0.75
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.75
1
0.25
0.25
0.5
0.75
Samples analyzed for this compound but not detected
Sample not analyzed for this compound
Detected below quantitation limit
GC/MS Analysis performed
EHNR/DEM LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 96-18-4 1,2.3-Trich!oropropene
u 108-86-1 Bromobenzene
u 95-49-8 2-Chlorotoluene
u 106-43-4 4-Chlmotoluene
u 541-73-1 1,3-Dichlorobenzene
u 106-46-7 1.4-Dichlorobenzene
0.51 95-50-1 1,2-0ichlorobenzene
u 96-12-8 1,2-Dibromo-3-Chloropropane
u 120-82-1 1.2,4-Trichlorobenzene
u 87-68-3 Hexachlorobutadiene
u 87-61-6 1,2,3-Trichlorobenzene
0.49 1634-04-4 Methyl-tcrt-butyl_ ether
u 71-43-2 Benzene
u 108-88-3 Toluene
u 100-41-4 Ethyl benzene
u 108-38-3 rn,p-Xylenes
u 95-4 7-6 a-Xylene
u 100-42-5 Styrene
u 98-82-8 lsopropy1benzene
u 103-65-1 n-Propy1benzene
u 108-67-8 1,3,5-Trimethylbenzene
u 98-06-6 tert-Butylbenzene
u 95-63-6 1,2,4-Trimethylbenzene
u 135-98-8 sec-Bulylbenzene
u 99-87-6 p-isopropyttoluene
u 104-51-8 n-Butylbenzene
u 91-20-3 Naphthalene
Gasoline Range Estimated Total Petroleum Hydrocarbon
Other pwgeables detected
(up to 1 O highest peaks)
NO VOLATILE ORGANIC COMPOUNDS
DETECTED BY GC/PID.
LAB NO. 6G1724
0.25 u
u
0.25 u
0.25 u
0.25 u
0.25 u
0.25 u
u
0.25 u
0.25 u
0.75 u
5 u
u
u
1 u
2 u
u
u
u
u
u
u
u
u
u
u
u
mg/l rng/l
0.25 N
Oe1ec1ed
ugll
.,.
COUNTY
QUAD NO
IREDHL
Rl:POR r TO ,,0t0R00c_ ________ Regional Office
COLLEC fOR(S) : ;l~lA~l~IL~E~N_:_ ______ _
rJA TE: 1##11#11111##
TIME·
PURPOSE
I AIIORATORY ANALYSIS ..
1100 )10
COl)Jligh 340
CUU Low JJ5
Coliform MF Fecal 31616
Coliform: MFT01alJlSO.t
IOC
1 u1biti1y
I-Re~idue , Suspended 530
r 01al Suspended soliJs
pll
,\lkalinity to pll ~-S
Alkalinity to pll 8.J
Carl,onale
Uica1bona!e
Carbon dioxide
Chloride
Clumnium Ile~ 10.12
('olm: ·1 rue 80
Cyanide 720
C01\11\IENTS:
mg.'L
mg!L
mg/L
1100ml
1100ml
mwl
N'IU
mg/L
mg/I.
u111ts
mg.IL
mg/L.
m~L
mg/L
mglL
mg/L
ug/1.
"'
mg.IL
Ownc1·
Location or Snc
Descrip1ion of sampling point
Sampling Method·
Remarks·
Disli Solids 70JOO
Fluoride 951
I lardness: to1al 900
I lardncss: (non·carb) <}()2
Phenols"J27JO
Specific Coml. 95
Sulfate
Sulfide 745
~111,\S
O,t n111J Orcn,c
Silica
Boron
NIIJ as N 610
TKN as N 625
X N02 tN03 as n 630
r. Total as P 665
1'04
DIVISION OF ENVIRONI\IENTAL l\lANAGEI\IENT
Chemitlry L11horntory Report/ Ground \\'11ler Qunli1,
SAMPLE PRIQRITY
□ROUTINE ~EMERGENCY
EJ CIIAJNOFCUSTODY
~ SAMPLE TYPE
177 LAURN DR STATESVILLE
mg/L
mgll.
mg/L
m!!}t.
ugil.
u~1hos1cm2
m;;/L
mg/I.
1ngl\.
mgll.
mg1t.
0.04 mg1L
mg.IL
1 S mglL
mg'L
mglL
□
Ag-Sih er 46566
,\I-Aluminum 46557
As-Arsenic 46551
Oa-Dariurn 46558
Ca-Calcium 46552
CJ-Cadiun1 46559
l"r-Chnuniu111 46560
Cu-Copper 1042
Fe-hon I04S
' Ilg-Me1c1uy 71'100
K-Potnssium 46555
Mg• '-1a;;ncsium '127
Mn-Manganc~ 1055
Na-Sodium 929
Ni-Nickel
Pb-Lead 46564
Se-Selenium
Zn_Zinc 46567
Lab Number 6G 1980
Date Received 9110/96
Time Rccei,·cd · 12:00 AM
Received By HMW
Released By OS
Date rcpor1ed : 10/21196
,g/L Organochlorine Pes1icides
,sfL Organophosphorus Pesticides
ug/L Nitrogen Pesticides
ug/L
mg/L Acid Herbicides
ug/L
,g/L Sernirnlatiles
,g/L TPH-Diesel Range
ug/L
1.3 ugll. X Vnln1ilc 011:(nnics (VO,\ honk)
rng/L
rng/L !"Pl I-Gasoline Ran;;e
ug/L rPII-UTEX Gasoline Range
mg/L
ug/L
uglL
ug/L
ugiL
6GIU0 SEP
__ .,.... t -..
\
GilOUNDWATER FIELD/LAB FORM
;_;; l.-f=.A5 J;;
;c1,,i >' H
COUilty .:r,:.e_J,d L
Quad No Lb 7,, 7 Serial No _______ _
Lal. :yS"l/.J., S"'B'~ong. eo. -!:>-e I Jy"l..v
BOD, 310
mg/I J)iss. Solids 70300 mg/I
--
COO High 340
mgtl Flou,ide 951
mg/I
-· COO Law 335
m~tl Hardness: Total 900 mg/L
Colilorm: MF Fecal 31616 1100ml Hardness {non-carb} 902 mgll
Colilorm: MF Talal 31504 1100ml Phenols 32730
ugtl
TOG 680
mgtl --Sgecific Cond. 95 uMhos/cm2
Turbidily 76
-NTU Sulfate 945
mg/I
Residue., Suspended 530 mglf Sulfide 745
mgtl
pH 403
unit~
Alkalinity lo pH 4.5 410 mgtl
Alkalinily to pH 8.3 415 mgll
Carbonale 445
mgll NH as N 610
mg!!_
Oicarbonale 440 mgll --JISl'LasJL62'
"'QIL
·---Cmbon dioxluo ~us 1111)11 ~ /<O,_;-NO, as N 630 mg!!_
Chloride 940
mgll P: Toial as P GG5
mg/I
--Chromium: Hex 1032 ug/1
Color: True oo Pl-Co
Cy~nido 720
mg/I
.....
.,X.
-
ltUl l/1 l....ill Vlllld
Oepartmenl of Environment, Hcallh, and Natural Resources
DIVISION OF ENVlflONMENTAL MANAGEMENT· GROUNDWATER SECTION
Lab Number 6 G-fl8{J
Date Recei,vpd 1to9!0 Time oq'.tO
Rec'd by: tth!Ju' From: Bus~, Hand Del.,
Other:-----~-----------
Data Entry By: ¥✓ Ck: _____ _
Dale Reported: --------------:::;:::..:c:·
·
:
:
·
-
:
:
;
:
·
-
-
.
_
_

Ag • Silver 46566
ugll --Organoch!orine Peslicides
Al • Aluminum 46557 ugll Organophosphorns Pesticides
As -Arsenic 46551
UQ/1 Nitrogen Pesticides
Ba -Badum 46558 ug!I
Ca • Calcium 46552 maj Acid Herbicides
Cd • Cadmium 46559 uqil
Cr -Chromium 46560 ugll --Semivolatile Organics
Cu • Cooner 46562
U!J}I
Fe . Iron 46563
ugll
H,1 • Mei curl 71900
ug/1 ·~ Volatile O1ganics (VOA bollle)
K • Potassium 46555 m[fl
Mg • Magnesium 46554 mg/I TPH • Gasoline Range
Mn • Manganese 46565 ug/I TPH · BTEX Gasoline Range
Na • Sodium 46556 mg/I
Ni· Nickel
ug/1
I 7
Pb . Lead 46564
ugtl •
Se • Selenium
ug!I "~
Zn · Zinc 4G5G7
ug!I \
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
75.35.4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-6&-3
74.97.5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-67-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18:-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79-34-5
TOL·
T-
E·
U•
N•,
I),
M-
WATER
1, 1-Dichloroelhene
0.75
Methylene Chloride
10
trans-1,2-0ichloroethen
e

0.75
1, 1-0ichloroethane
0.25
2,2-0ichloropropa.ne
0.25
cis-1,2-Dichloroethene
0.25
Chloroform
0.25
Bromoch!oromelhane
0.75
1.1. 1-Trichloroelhane
0.25
1, 1-0ichloropropene
0.25
Carbon Tetrachloride
0.75
1,2-Dichloroethane
0.25
Trichloroelhene
0.25
1,2-0ichloropropane
0.25
Bromodichloromethc1ne
0.25
Oibromome!hane
cis-1, 3-□ichloropropene
0.25
trans• 1, 3-Dichloropropene
0.25
1, 1,2-Trichforoethane
0.25
Te!rachtoroethene
0.25
1.3-Dichloropropane
0.25
Oibromoch!oromethane
0.75
1,2-0ibromoethane
1
Chlorobenzene
0.25
1, 1, 1,2-Tetrachloroethane
0.25
Bromoform
0.5
1, 1,2,2-Tetrach!oroethane

0.75
Target Ouantilalion Limil-Subject to
change due to Instrument sensitivity
Tenlalively ldenlifiecf, not confirmed
Esllma!ed Value
Samples analyzed for this compound bu! not detected
Sample not analyzed for this compound
Oeler,lijd helow quanlilalion limit
OCIMB A11nly11la p~1frn111ttd
EHNRIDEM LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 96-18-4 1,2,3-Trichloropropane
u 108-86-1 Bromobenzene
u 95-49-8 2-Ch!orotoluene
12
106-43-4 4-Chlorolo!uene
u 541-73-1 1,3-0ichlorobenzene
3.4 ET
106-46-7 1,4-Dichloroben2ene
u 95-50-1 1,2-0ichloroben2ene
u 96-12-8 1, 2-Dibromo-3-Chloroprop
a
n
e

u 120-B2-1 1,2, 4-Ttich!orobenzene
u 87-68-3 Hexach!orobutadiene
u 87-61-6 1,2, 3-Trichlorobenzene
0.53
1634-04-4 Methyl-lert-butyl elher
u 71-43-2 Benzene
u 108-88-3 Toluene
u 100-41-4 Ethyl benzene
u 108-38-3 m,p.Xylenes
u 95-47-6 o-Xy!ene
u 100-42-5 Styrene
u 98-82-8 lsopropylbenzene
u 103-65-1 n-Propylbenzene
u 108-67-B 1,3,5-Trimethy!benzene
u 98-06-6 tert-Butylbenzene
u 95-63-6 1.2,4-Trimethy!benzene
u 135-98-B sec-Butylbenzene
u 99-87-6 p-isopropylloluene
u 104-51-8 n-Butylbenzene
u 91-20-3 Naphthalene
Gasoline Range Estimated Total Pe!roleum Hydrocarbon
Other purgea.bles de!ecled
(up to 10 highest peaks)
NO VOLATILE ORGANIC COMPOUNDS DETECTED BY
GCIPID.
LAB NO. 6G1980
SUPERVISOR~
DATE~
ENTEREDB .
DATE -• 1/7
0.25 u
' u
0.25 u
0.25 u
0.25 u
0.25 D
0.25 u
u
0.25 u
0.25
u
0.75 u
5 u
u
u
1 u
2 u
u
u
u
u
u
u u
u
u
u
u
mg/L mg/L
0.25 N
Delected
ugll
COUNTY
QUAONO:
IREDEI.L 96 SF.P ! 7 PH 2= O!i
REPORT TO O,_1R~O~~-------Rcgional Office
COU.ECTOR(S) · _D_A_I_IL_E_'N _______ _
ll,\TE: 7/30196
llME:
PlJRPOSl::
LABOIUTORY ANALYSIS
DOD Jt0
COD lligh 340
COD I.ow JJ5
Coliform: MF Fecal 11616
Coliform: MFTo!JIJ1504
roe
furbitity
Residue., Suspend.-d 5)0
J"o1al Suspended solids
pl I
,\llolimty 10 r,114.5
Allalinity to pll 8.J
Car Ix.mate
llicarbonal<"
C"arl,on dio~ide
Chlmide
Chromium lk"< l0J!
Color: Tru<' 80
Cyanide 720
mg/L
mg/L
mg.II.
1100ml
1100ml
mg)l
NlU
mg/L
mglL
uni!s
rngl\.
mg/L
mg/L
mg.IL
mgll.
mglL
u£1L
'" mg,L
Owner:
l.0<:alion or Siie:
O,:scrir,1ion ofsamplin!! point
Smnr,lin!! ldc!hnd
Rema,1-,s
Diss Solids 70300
Fluo,ide 951
I b,dness. total 900
I lardnen: (non-ca,b) 90:?
Phenols 32730
Specific Cond " Sulfate
Sullide 745
1--llJAS
Oil and Grease
Silirn
Boron
NID as N 610
TKN as N 625
NO2 tNOJ asn hl0
P. Totalasl'663
PO4
l>l\'ISION OF EN\'IRON/\IENTAL 1\IANAGE/\IENT
Ch.-mi1try l.11bon11ory Rrro~I I Grnund W111n Q1111li1y
SAMl'!,E l'RIORITY
E)ROUTINE
(D CIIAINOl'CUSTODY
@] SAMPLE TYPE
□EMERGENCY
□
DA\"IDSON ROOFING HENTt\1.111/(;ES WELL
mgll Ag-S,her 46566
"'!!IL Al-,\luminum 46557
mglL As-A,senic 46551
ing.'l. \la-Barium 46558
•gll C"a·Calcium 46551
uMhos/cm! Cd-Cadium 46559
mg/L Cr-Chromium 46560
mg/L Cu-C"or,pc, 1042
m!c!IL Fe• lrn11 1045
mg.IL I lg-Mc,cury 71900
"'!l'l. K-l'ul;1Hium ·16555
M!t,• 1--lagnc,ium 'l27
Mn-Manganese 1055
mg•l. Na-Sodium 929
mg/L Ni-Niclcl
m~1l. l'h-l.cad fo5t, I
mgll. Sc-Selenium
mg•L Zn_Zinc 4b567
Lab Number 6(;1649
Dale Recei,·,:d 7fJ 1196
Time Recei'"ed 9:30 AM
Rccei'"ed Dy OS
Released ny OS
Date rcpor1ed : 960828
•g/L X Oq;anochlorine Pesticides
.. y1. X Organophosphorus rcslicidcs
u!:lfL Nitrogen Pesticides
uglL
mglL Acid I ie1bicides
•gll
ug/L Semi,·olati!cs
ug/1. fl'II-Dicsel Range
ug/L
ug/L X Volatile O,ganics (VOA bonleJ
mg/I.
mgll. 1'1'11-Gasohue Range
ug/1. fl'II-BTEX Gasoline Range
mg.IL
uglL
uglL
ug.11.
ugll.
,, North Carolina
GROUNDWATER FIELD/LAB FORM Department of Environment, Health, and Natural Resources
DIVISION OF ENVIRONMENTAL MANAGEMENT-GROUNDWATER SECTION
County -r,.. e,./.,,,tl
Quad No LI..'"" Serial No. ______ _
CHAIN OF CUSTODY
Lat. iJ-0 ·r.). '~-I'" N Long. <';'o "~-7, Sv'' lJ
SAMPLE PRIORITY 0
IZJROUTINE □EMERGENCY
,.-;,:;;:;i 'E:)CHAIN OF CUSTODY
Report To: ARO, FRO.~, ARO, WaRO, WiRO,
WSRO, Kinston FO, Fed. Trust, Central OIi., Other: ________ _
Lab Number -~~2,~~.::l..!.~~-~=---
Date Recei".'v!!!!.-:1-Ji==-'CLI . ...Li-l-l.-
Rec'd by::_ -l>-L.-= rom: us oune an Del.,
Other: _________________ _
Data Ent,y By:. ______ Ck: _____ _
Date Reported: ______________ _
Shipped by: BuS,(~Uri r, Hand Del., Other_·------------,,-·-Purpose: ;
Collector(s): j)c k "o, Date --z/Jo /'?(, Time 05'.') 5 Baseline Complai ,..Compliance, LUST. Pesticide Study, Federal Trust, Other: _______ _ r I I "''----• . ,...., \Clltll one) / FIELD ANALYSES ; 7< Owner c.v1 "1 "" • .., • c I
pH -r-:" Spec. Cond.94 Lff at.25" C Location or site --------,--,--------,------------------
Te~~-,o -~~,.-,---0 c Odor __ -_____ Description of sampling point -~fc,,?'ce'_,-1i~·uc...c{,__~c~,'-~~w::=~4~&=<~.J~------------------
Appearance c &sc/<:c[< C:,__,, Sampling Method ------~,,_~~-i,._~,,.~,,~ .. ~,i~-------Sample Interval, _______ _
Field Analysis By: ---'O=c~l.,_J.,_1t_________ Remarks-----------------~~-----------------(pump111o bme, 1ir tamp. lie.)
LABORATORY ANALYSES
BOD. 310 mcil Diss. Solids 70300 mg/I Aa -Silver 46566 un,I --.,...-Oraanochlorine Pesticides
COD High 340 mg/I Flouride 951 mnll Al• Aluminum 46557 uail 19 Organophosphorus Pesticides
COD Low 335 m~I Hardness: Total 900 mg/I As -Arsenic 46551 u9!!. Nitroaen Pesticides --Coliform: MF Fecal 31616 1100ml Hardness tnon-carb\ 902 m-'I Ba -Barium 46558 un.l
Colilorm: MF Total 31504 /100ml 0 "enols 32730 unn Ca -Calcium 46552 mn/1 Acid Herbicides
TOC 680 m(J/1 Sgecilic Cond, 95 uMhos/cm2 Cd -Cadmium 46559 und
Turbidity 76 NTU Sulfate 945 mntl Cr -Chromium 465G0 un.l Semivolatile Oraanlcs
Residue., Suspended 530 mg/I Sulfide 745 mnll Cu -Conner 46562 urul
Fe -Iron 46563 urn I
Hq -Mercury 71900 un/1 >< Volatile Organics (VOA bottle)
pH 403 units K -Potassium 46555 ma/I
Alkalinity to pH 4.5 410 mg/I Ma -Magnesium 46554 mg/I TPH -Gasoline Range
Alkalinity to pH B.3 415 mg/I Mn -Mannanese 46565 unll TPH -BTEX Gasoline Range
Carbonate 445 mg/I NH as N 610 mn.l Na -Sodium 46556 , mg/I
Bicarbonate 440 mail I TKN --IL62' mgtj_ Ni• !'lickel ug/1 , )
Carbon dioxide 405 mq/1 NO +NO as N 630 mnn Pb -Lead 46564 untl 1/
Chloride 940 . mg/I P: Total as P 665 mail Se -Selenium unll \I
Chromium: Hex 1032 ug/1 Zn -Zinc 46567 unn
Color: True eo Pt-Co
Cyanide 720 mg/I
Lab Comments:-----------------------------------------------------------
GW-54 REV "'93 For Dissolved Analysis -submit filtered sample and write .. DIS" in hlr·•-
\___..
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
75-35-4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79.34.5
TOL-
T-
E-
U-
N-
D-
M-
COMMENTS:
WATER
1, 1-Dichloroethene 0.75
Methylene Chloride 10
trans-1,2-Dichloroelhene 0.75
1, 1-0ichloroethane 0.25
2,2-Dichloropropane 0.25
cis-1,2-Dichloroethene 0.25
Chloroform 0.25
Bromochloromethane 0.75
1.1, 1-Trichloroethane 0.25
1.1-Dichloropropene 0.25
Carbon T etrachforide 0.75
1,2-Dichloroethane 0.25
Trichloroethene 0.25
1.2-Dichloropropane 0.25
Bromodichloromethane 0.25
Dibromomethane 1
cis-1,3-Dichloropropene 0.25
trans-1,3-Dichloropropene 0.25
1, 1,2-Trichloroethane 0.25
T etrachloroe\hene 0.25
1,3-Dichloropropane 0.25
Oibromochloromethane 0.75
1, 2-Dibromoethane 1
Chlorobenzene 0.25
1, 1, 1.2-Tetrachloroethane 0.25
Bromoform 0.5
1, 1,2.2· T etrachloroethane 0.75
Target Quantilalion limit-Subiect to
cllange due lo instrument sensitivity
Tentatively Identified, nol confirmed
Estimated Value
Samples analyzed for this compound but not delecled
Sample not analyzed for this compound
Detected below quanlilation limit
GC/MS Analysis performed
EHNR/DEM LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RES UL TS
u 96-18-4 1.2,3-Trichloropropane
u 108-86-1 Bromobenzene
u 95-49-8 2-Ch!oro!otuene
u 106-43-4 4-Chlorololuene
u 541-73-1 1, 3-Dichlorobenzene
u 106-46-7 1,4-0ichlorobenzene
0.95 95-50-1 1,2-Dichlorobenzene
u 96-12-8 1,2-Dibromo-3-Chloropropane
u 120-82-1 1.2. 4-T richlorobenzene
u 87-68-3 Hexachlorobutadiene
u 87-61-6 1.2.3-Trichlorobenzene
u 1634-04-4 Melhyl-tert-butyl ether
u 71-43-2 Benzene
u 108-88-3 Toluene
u 100-41-4 Elhyl benzene
u 108-38-3 m,p-Xylenes
u 95-47-6 a-Xylene
u 100-42-5 Styrene
u 98-82-8 lsopropylbenzene
u 103-65-1 n-Propylbenzene
u 108-67-8 1,3.5-Trimethylbenzene
u 98-06-6 lert-Butylbenzene
u 95.53.5 1,2,4 -Trirnethylbenzene
u 135-98-8 sec-Butylbenzene
u 99-87-6 p-isopropylloluene
u 104-51-8 n-Butylbenzene
u 91-20-3 Naphthalene
Gasoline Range Estimated Total Petroleum Hydrocarbon
Other purgeables detected
(up to 10 highest peaks)
LAB NO. 6G1649
ENTERED BY
DATE
0.25
1
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.75
5
2
mg/L
0.25
10
3.0
12
19 E
7.7 E
17 E
4.7
3.3
mg/L
Detected
ug/L
SEVERAL UNIDENTIFIED PEAKS DETECTED BY GC/PID.
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
N
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
15972-60-8
309-00-2
1912-24-9
JI 9-84-6
319-85-7
319-86-8
58-89-9
57-74-9
5103-71-9
5103-74-2
3734-48-3
2675-77-6
501-15-6
2921-88-2
1897-45-6
1861-32-1
53-19-0
72-54-8
3424-82-6
72-55-9
789•02-6
50-29-3
60-57-1
959-98-9
)3213-65-9
1031-07-8
50594-66-6
25057-89-0
133-90-4
94-75-7
94-82-6
1918-00-9
51-36-:'"
CGY
VA JA
KAK \</\1'-'
WATER
ALACHLOR
ALDRIN
ATRAZINE
BJIC-ALPIIA
BIIC-BETA
BIIC-DELTA
81/C.GM.IMA(UNDANE)
CHLORDANE, TECHNICAL
CIILORDANE-ALPIIA
CIILORDANE-GAMMA
CIILORDENE
CIILORNEB
CIILOROBENZILATE
CIILORPYRIFOS
CIILOROTHALONIL
DCPA
DOD, or
DOD, PP
DOE, OP
DOE, PP
DDT, OP
DDT. PP
DIELDRIN
ENDOSULFAN I
ENDOSULFAN II
ENDOSULFAN SULFATE
ACIFLUORFEN (BLAZER)
BENTAZON
CHLORAMBEN
2,4-0
2,4-DB
DCPA (ACID METABOLITES)
DICAMBA
3,5 DICHLOROBENZOIC ACID
EHNR/DEM LABOR A TORY PESTICIDES ANALYTICAL REPORT
ANALYSIS RESULTS
0.10 u 72-20-8 ENDRIN
0.08 u 7421-93-4 ENDRIN ANDEHYDE
0.75 u 53494-70-5 ENDRIN KETONE
0.02 u 2593-15-9 ETIIAZOLE
0.03 u 76-44-8 1/EPTACIILOR
0.0J u 1014-57-3 1/EPTACIILOR EPOXIDE
0.01 II 118-74-1 ll EXACIILOROllENZENE
O.JO u 121-75-5 ~1ALATIIION
0.02 \J 72-43-5 METIIOXYCIILOR, PP
().(JJ u 2]85-85-5 MIREX
O.fll II JQ765-80-5 TRANS-NONACIILOR
(l.()J u 26880-48-8 OXYCIILORDANE
5.00 II 52645-5)-1 MIXED-PERMETIIRIN
0.08 \l 19111-16-7 PROPACIILOR
0.03 u 117-18-0 TECNAZENE
0.02 u 1582-09-8 TRIFLURAUN
0.06 II 12674-11-2 AROCJILOR 1016
0.04 u 11104-28-2 AROCl!LOR 1221
0.05 u 11141-16-5 AROCIILOR 1232
0.02 u 53469-21-9 AROCHLOR 1242
0.04 u 11071-29-0 AROCllLOR 12411
0.06 u 11097-69-1 AROCflLOR 1254
0.02 u I 1096-82-5 AROCHLOR 1260
0.03 u )7324-23-5 AROCIILOR 1262
0.01 u 8(Xll-J5-2 TOXAPIIENE
0.02 u UNlllENTIFIED PEAKS DETECTED
D
0.50 N 120-36-5 DICIILORPROP
5.00 N 88-85-7 DINOSEB
0.50 N 7600-50-2 5-IIYDROXYDICAMBA
1.60 N 100-02-7 4-NITROPIIENOL
5.00 N 87-86-5 PENTACIILOROPIIENOL (PCP)
0.36 N 1918-02-1 PICLORAM
{l.]5 N 93-76-5 2.4,5-T
0.50 N ·.72.J 2,4,5-TP (SIL VEX)
UNIDENTIFIED PEAKS DETECTED
LAB NO. 6G 1649
SUPERVISOR K-11 \<'....
DATE_~li>J.:Jj.u.,/0~<--
~ti/90
ENTERED BY
DATE
O.oJ
0.05
0.04
0.03
0.02
0.01
0.01
{UJ8
0.05
0.03
0.02
0.02
1.00
0.10
0.02
0.03
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
1.50
8.50
0.40
2.00
4.00
0.30
1.00
0.75
1.50
u
u
u
u
lJ
u
u
u
\J
u
u
\J
\J
\l
\J
\J
\J
\J
u
u
\J
u
u
u
u
N
N
N
N
N
N
N
N
LAB II
PESTICIDES REPORT -DEM LAB PAGE 2
ORGANOPHOSPHATE PESTICIDES BY FLAME PHOTOMETRIC DETECTION
786-19-6 CARBOPIIENOTIIION
2921-88-2 CHLORPYRIFOS
50-29-3 DEF
298-03-3 DEMETON
333-41-5 DIAZINON
62-73-7 DICllLORVOS
60-51-5 DIMETHOATE
298-04-4 DISULFOTON
2497-06-5 DJSULFOTON SUISONE
2497-07-6 DISULFOTON SULf-OXIDE
2104-64-5 EPN
563-12-2 ETIIION
131 94-48-4 ETHOPROP
15972-60-8
834-12-8
1912-24-9
314-40-9
23184-66-9
2008-41-5
5134-68-5
101-21-3
1134-23-2
2921-88-2
333-41-5
957-51-7
759-94-4
22224-92-6
51235-04-2
51218-45-2
ALACIILOR
AMETRYN
ATRAZINE
BROMACIL
BUTACHLOR
BUTYi.ATE
CARBOXJN
CHLORPROPHAM
CYCLOATE
CIILORPYRIFOS
DIAZINON
DIPltENAMID
EPTC (EPTAM)
FENAMIPIIOS
llEXAZINONE
METOLACIILOR
TOL-Target Ouantitation Limit-Subject to
change due to instrument sensitivity
T-Tentatively_ Identified, not confirmed
E-Estimated Value
1.0 u
I.I u
2 5 u
2.5 u
0.8 u
2.1 u
3.5 lJ
1.0 lJ
2.3 ll
NE u
4.0 u
u ti
2.0 u
3.4 N
I.I N
0.8 N
3.4 N
4.8 N
2.2 N
6.5 N
4.2 N
2.4 N
1.0 N
0.5 N
2.8 N
2.3 N
1.2 N
5.1 N
4.2 N
55-38-9 2.0
I 15-9C}-2 FENSULFOTHION 10.0
150-50-5 FOLEX 2.0
6923-22-4 MEVINPHOS 1.9
300-76-5 MONOCROTOPHOS JO.O
56-38-2 NA LED 4.0
29fl-(X).(J ETIIYL PARATIIION 0.7
298-02-2 METIIYL PARATIIION 1.5
299-11-1-3 PllORATE 1.5
3689-24-5 RONN EL 0.8
1307 I-74-9 SlJLFOTEPP 0.3
7786-],1-7 TERBUFOS I. I
UNIDENTIFIED PEAKS DETECTED
2I087-M-9 METRIBUZIN 1.6
113-48-4 MGK264 5.1
2212-67-1 MOLINA TE 2.1
15299-99-7 NAPROPAMIDE 2.6
27314-13-2 NORFLURAZON 7.1
1114-71-2 PEBULATE 6.7
1!110-IM-O l'ROt-lETON 2.5
7287-19-6 PROMETRYN 2.4
23950-58-5 PRON AMIDE 7.6
I 39-40-2 PROPAZINE 1.0
122-34-9 SIMAZINE I. I
I0\4-70-6 SIMETRYN 2.2
34014-18-1 TEBUTHIURON 3.1
5901-51-2 TERflACIL 4.4
886-50-0 TERBUTRYN 1.4
1929-77-7 VERNOLA TE 0.6
UNDIENTIFIED PEAKS DETECTED
N· Sample not analyzed for this compound
D· Detected below quantitation limit
NE• No established TQL
U-Samples analyZed for this compound but not detected
6G1649
u
u
u
u
u
u
u
u
u
u
u
lJ
0
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
COMMENTS:------------------------------------------------
COUNTY
QUAD NO
IREllELI.
REPORTlO
COLLECTOR{SJ
DATE:
c~c\c",c~c,.c>:cN~-------Rcgio.,al Onicc
7/J0/96
TI:-.!!:
PUil.POSE:
LABORATORY ANALYSIS
RODJIO
COD l!,ghJ40
COD Low 335
Coliform· :,,.\f F.-cal 31616
Coliform· MF Total] 150-1
TOC
1"urbi1i1,-
Rc~iduc . Su~pendcd 530
Total Suspended solids
pll
,\ll:ilinity W r114 S
Al~alinily to pH 8 J
Carhonaie
llica<l>onale
Carl>or, di,;"idc ,
Chloride
(hron1ium: lie~ 10.12
ColN: T1ue SO
Cyanide 7:0
CO,\l,\IE,'\'.TS:
mg/I.
mf)L
m~L
1100ml
1100ml
mgll
NTU
mJ!}L
rngll.
um1l.
n,glL
m~_IL
mg/L
mgl\,
mg.IL
m;:/L
ug1L
'" mgll.
O"ncr:
Location or S11c
Dcscrip1iu" ofsan1pli11;; poi11t
Sampling Method·
Rcm;u~s·
OiH. Solids 70300
Fluo1idc951
I la,dncss: total 900
1 lmdncn: (non-carb) 902
l'l,cnol'> 327.10
Specific ComJ. 'l5
Sulfate
Sulfide 7~5
~IBAS
Oil nnd Gre;isc
Silica
Boron
NIU JS N 610
rKN as N 625
N02 +NOJ as 11 630
r: Tut;il as P 6GS
1'04
IH\'ISION OF EN\'IRON;\IENTAL M,\NAGE;\IENT
Chtmis!ry Labonlol") lfrporl / Gnrnrul WHlcr QuHlil)
SM1PLE PRIORITY
E]ROUT!NE
El CIIA!NOFCUSTODY
~ SAMPLE TYl'E
lllHJCE F.l.,\10RE
mg/I.
m,g.lL
mg.IL
rng/L
u!;JL
u:,,.lhos/cm2
m!UL
mg/L
mg/L
mglL
mg/L
mg'L
m,.IL
m;,JL
mg/L
mglL
□
,\!,'.-Sil"cr ~6566
Al-Aluminum .\6557
As-Arsenic 46551
lla-lfarium 46558
Ca-Calcium 46552
Cd-Cadium 4Ci559
Cr-("hromiu111 465(i0
Cu-Copper ion
Fe-lroo 1045
1 lg-Mercury I 1900
K-l'(,1a,siu111 -1r,555
'-lg-,\fagnesium 927
Mn-M11ng11ncsc 1055
Na-Sodium 929
Ni-Nidcl
l'b-1.cml 465Ci4
Sc-Sckniu111
Zn Zioc 46567
U.\VI.
ug,11.
ug'l.
ugll.
rn)'.IL
ug/L
U!(IJ.
u!!fl.
ug.ll.
11;:'l.
11\)1.1[.
111!,11.
U!!,,~-
mg/L
u!'-'L
u~1l.
ugll_
ug.•1.
I.ab N111nbt-r
lla1c Rccci,cd
1 imc Rccci, cd
Rccci,cd Br
I 1'11-ll,nel R1111gc
11'11-(ias.,lone lt11ngc
! 1'11-111 E.'>: {i.Jso1,ioe Ran!/~
CiG16-Hi
7/Jlfq6
'l JO AM
DS
North Cnrollnn
GROUNDWATER FIELD/LAB FORM Department of Environment, Honlth, end Natural Resources
DIVISION OF ENVIRONMENTAL MANAGEMENT. GROUNDWATER SECTION -County_=,,-"""'--"-il.-----------
Ouad No L 67"" Serial No. ______ _
Lat. 3 5°0 'r;;,.' S°'? 1NLong. 8,/-;-,~ · "Y' LJ
Report To: ARO, FRO~ RRO, WaRO, WiRO,
• V
SAMPLE PRIORITY
[g'ROUTINE · □EMERGENCY
[;2jCHAIN OF CUSTODY _
WSRO, Kinston FO, Fed. Trust, Central OH., Other: ________ ~
Shipped by: Bus,~-Hand Del., Other_· ___________ _
0
Lab Number -1..>LJ,,,;;:c~~-'--"----=--~-=----
F-l+.L._Tim~ 9: 50
Rec'd by:_-"'--6,.....L.__ Froni: Bus,@, Hand Del.,
Other:
Data Entry By: ______ Ck: ______ _
Date Reported: _____________ _
. ~ 7? L Purposo: ,-~ Collector(s): ·j)c l,\ '°" Date ~ ~7u~1'?L~~-~--Time 0 '?: 2 S -Basoli11o(CornplninI_,,Complianco, LUST, Posticido Study, Fodornl Trust, Othor: ______ _
/ ------------\Ci!CIII 0/0ll) FIELD ANALYSES -,,_) owner t:. ....-<...
pH,00 ~,-:.o Spec.Cond.94 'tS al-25"C Locationorsite c,·:i.. /c,_,c<,,,,-J).-c,-,C, ){d~c~,ll,,, ,)__eG77
Temp.10 , _ 0 c Odor ,., ~ ( Description of sampling point ~etsd c= b'".' C. )'°0 -\.-l :n c7Sc'i «' Zi ✓
Appearance....,:c;..C~<,,~""'r-~----------Sampling Method -------.,.~--,,..,..,-~--------Sample Interval _______ _ I { (~1lor,11lc) Field Analysis By: c b12 Remarks c:{ ..-t__ --Co
LABORATORY ANALYSES (pumpinQ t1m11, air lamp. ate.) •
BOD, 310 mq/1 Diss. Solids 70300 mrul Aa • Silver 46566 uo/I ~ Or~anochlorine Pesticides
COD High 340 mg/I Flouride 951 mail Al • Aluminum 46557 uatl Organophosphorus Pesticides
COD Low 335 mg/I Hardness· Total 900 mail As• Arsenic 46551 unil Nitrooen Pesticides
Coliform: MF Fecal 31616 1100ml Hardness (non-carbl 902 mail Ba -Barium 46558 uq/I
Coliform: MF T olal 31504 /100ml Phenols 32730 uail Ca • Calcium 46552 ma/I Acid Herbicides
TOG 660 mqtl Soecific Cond. 95 uMhos/cm2 Cd • Cadmium 46559 uoil
T urbidily 76 NTU Sulfale 94S mail Cr -Chromium 46560 uail Semivolatile Organics
Residue., Suspended 530 mg/I Sulfide 745 mClll Cu -Coooer 46562 uqtl
Fe -Iron 46563 uqtl
' Hg• Mercury 71900 ugtl I.X.. Volatile Organics (VOA bottle)
pH 403 unit~ K -Potassium 46555 mail
Alkalinity to pH 4.5 410 mg/I Mq -Maqnesium 46554 mqll TPH -Gasoline Range
Alkalinity to pH 8.3 41S mgil Mn -Manaanese 46565 uoil TPH · BTEX Gasolino Range
Carbonate 445 mgll NH -as N 610 mnn Na -Sodium 46556 mail
Bicarbonate 440 mail It<:~ as~ 625 rngLI Ni· Nickel ug/1
Carbon dioxide 405 mgil NO + NO as N 630 moil Pb -Lead 46564 uqil \ I JI./
Chloride 940 mg/I P: Total as P 66S mQ/I Se -Selenium uoil \ I I
Chromium: Hex 1032 UQ/1 Zn• Zinc 46S67 uail
Color: True BO Pt-Co
Cyanide 720 mg/I
Lab Comments: ---------------------------------------------------------
GW-S4 REV ""3 For Dissolved Analysis -submit filtered sample and write "DIS" in blr · '·
·-
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
75-35-4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79-34-5
TOL-
T-
E-
u-
N-
0-
M-
COMMENTS:
WATER
1. 1-Dichloroethene 0.75
Methylene Chloride 10
trans-1,2-Dichloroethene 0.75
1, 1-0ichloroethane 0.25
2, 2-Dichloropropane 0.25
cis-1,2-Dichloroethene 0.25
Chloroform 0.25
Bromochloromethane 0.75
1, 1, 1-Trichloroethnne 0.25
1, 1-Dichloropropene 0.25
Carbon Tetrachloride 0.75
1, 2-0ichloroethanc 0.25
Trichloroethene 0.25
1,2-0ich!o1opropane 0.25
Bromodichloroinelhane 0.25
Oibrornomett1ane
cis-1,3-0ich!oropropene 0.25
trans-1,3-0ich!oropropcne 0.25
1, 1, 2-Trichtoroctharie 0.25
Tetrachloroethene 0.25
1,3-Dichloropropane 0.25
Dibrornoch!oroniethane 0.75
1,2-0ibromoethane 1
Chlorobenzene 0.25
1, 1, 1,2-Tetrachloroetharie 0.25
Brornoform 0.5
1, 1,2,2-Tetrachloroethane 0.75
Target Ouantitation Limit-Subject to
change due to ins,trument sensitivity
Tentatively Identified, no! confirmed
Estimated Value
Samples analyzcd:for this compound but not detected
Sample not aria!y~ed for this compound
Detected below quantitation limit .
GC/MS Analysis performed
EHNR/DEM LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 96-18-4 1,2,3-T richloropropane
u 108-86-1 Bromobenzene
u 95-49-8 2-Chlorotoluene
u 106-43-4 4-Chloroto!uene
u 541-73-1 1,3-0ichlorobenzene
u 106-46-7 1,4-0ich!orobenwne
0.68 95-50-1 1,2-0ichlorobenzene
u 96-12-8 1,2-Dibromo-3-Chloropropane
u 120-82-1 1,2,4-Trichlorobenzene
u 87-68-3 Hexachlorobutadiene
u 87-61-6 1,2,3-Trichlornbenzene
u 1634-04-4 Me1hyl-tert-butyl ether
u 71-43-2 Benzene
u 108-88-3 Toluene
u 100-41-4 Ethyl benzene
u 108-38-3 m,p-Xy!enes
u 95-47-6 a-Xylene
u 100-42-5 Styrene
u 98-82-8 lsopropylbenzene
u 103-65-1 n-Propylbenzene
u 108-67-8 1 ,3,5-T rimethylbenzene
u 98-06-6 tert-Butylbenzene
u 95-63-6 1,2,4-T rimethylbenzene
u 135-98-8 sec-Butylbenzene
u 99-87-6 p-isopropyltotuene
u 104-51-8 n-Butylbenzene
u 91-20-3 Naphthalene
Gasoline Range Estimated Total Petroleum Hydrocarbon
Other purgeables detected
(up to 1 O highest peaks)
NO VOLATILE ORGANIC COMPOUNDS DETECTED BY
GC/PID.
LAB NO. 6G1648
0.25 u
1 u
0.25 u
0.25 u
0.25 u
0.25 u
0.25 u
1 u
0.25 u
0.25 u
0.75 u
5 u
u
1J
1 1J
2 u
u
u
u
u
u
u
u
u
u
u
u
mg/L mg/l
0.25 ''
Oe1ected
ug/L
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
15972-60-8
309-00-2
1912-24-9
319-84-6
319-85-7
J 19-86-8
58-89-9
57-74-9
5103-71-9
5103-74-2
)734-48-3
2675-77-6
501-15-6
2Q.2!-R8-2
1897-45-6
J 86!-32-1
53-!9-0
72-54-8
3424-82-6
72-55-9
789-01-6
50-29-3 .
60-57-l
959-911-9
33213-65-9
!031-07-8
50594-66-6
25057-89-0
-133~90-4
94-75-7
94-82-6
1918-00-9
51-36-{~
~,
CGY
VA VA
KAK 1<W
WATER
ALACIILOR
ALDRIN
ATRAZINE
BIIC-ALl'IIA
Bl!C-llETA
BHC-DELTA
I\IIC-G,\MM,\{UN DANE)
CI\LORDANE, TEC!INJCAL
CJILORDANE-ALPIIA
Cl!LORDANE-GAMMA
Cl!LORDENE
Cl!LORNEB
CIILOROBENZJLATE
Cl !LORPYRI rns
CIILOROTIIALONIL
DCPA
DDIJ,OP
DDD, PP
DOE.OP
DOE. PP
DDT, OP
DDT, PP
DIELDRIN
ENDOSULFAN I
ENDOSULFAN II
ENDOSULFAN SULFATE
ACIFLUORFEN {BLAZER}
BENTAZON
Ci!LORAMBEN
2,4-D
2,4-DB
DCPA {ACID METABOLITES)
DICM,H1A
3.5 DICl!LOROBENZOIC ACID
EHNR/DEM LABO RA TORY PESTICIDES ANAL YT I CAL REPORT
ANALYSIS RESULTS
0.10 u 72-20-8 ENDRIN
0.08 u 7421-93-4 ENDRIN ANDEHYDE
0. 75 u 53494-70-5 ENDRIN KETONE
0.02 u 2593-15-9 ETIIAZOLE
O.OJ u 76-4,\-8 JIEl'TAC!ILOR
0.0.l IJ 1024-57-3 llEl'TACHLOR EPOXJDE
0.()1 u 11 R-74-! II EXACI ILOROIJENZENE
U.JU u 121-75-5 MALATIIION
0.02 u 72-43-5 METHOXYCIILOR, PP
0.03 u 2385-85-5 M!REX
0:02 u 39765-80-5 TRANS-NONACJILOR
0.03 u 26880-48-8 OXYCIILORDANE
5.00 u 52645-53-l MIXED-PERMETIIRIN
0.08 u I 9! 8-16-7 PROPACIILOR
0.03 u I 17-18-0 TECN,\ZENE
0.02 u !5112-09-11 TRlf'LURALIN
0.06 u 12674-11-2 AROCIILOR 1016
0.0·1 u 11104-28-2 AROCIILOR 1221
0.05 u l l l4l-16-5 AROCHLOR 1232
0.02 u 53469-21-9 AROCIILOR l 242
O.O•l u 12672-29-6 AROCIILOR 1248
0.06 u 11097-69-1 AROCIILOR 1254
0.02 u I 1096-82-5 AROCHLOR 1260
0,03 u 37324-23-5 AROCIILOR 1262
0.01 u 8001-35-2 TOXAPHENE
0.02 u UNIUENTIFIEU l'EAKS DETECTED
AC RBI BY LECTRO CAPTU DETECTION
0.50 N 120-36-5 DICIILORPROP
5.00. N 88-85-7 DINOSEB
0.50 N 7600-50-2 5-IIYDROXYDICAMBA
1.60 N 100-02-7 4-NITROPIIENOL
5.00 N 87-86-5 PENTACJILOROPJIENOL (PCP}
0.36 N 1918-02-! PICLORAM
0.35 N 93-76-5 2,4,5-T
0.50 N \-72-1 2,4,5-TP (SIL VEX)
UNIDENTIFIED PEAKS DETECTED
LAB NO.
SUPERVISOR
DATE
ENTERED BY
DATE
0.0J
0.05
IUH
(l.(JJ
(l.02
\l.()t
ll.OI
II.OH
0.05
0.0.l
0.02
0.02
1.00
ll_!O
11.02
0.0J
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
1.50
8,50
0.40
2.(XJ
4.U<J
O.JU
1.00
0.75
1.50
DETECTED·
.',\•·:\j•/L
u
u
II
u
II
I/
II
I/
IJ
IJ
u
u
IJ
I/
II
u
IJ
u
u
I/
I/
u
u
u
u
N
N
N
N
N
N
N
N
LAB I/
PESTICIDES REPORT -DEM LAB PAGE 2
ORGANOPHOSPHATE PESTICIDES BY FLAME PHOTOMETRIC DETECTION
786-19-6 CARBOPIIENOTl!!ON
2921~8S-2 CHLORPYRJFOS
50-29-3 DEF
29S-0J-3 DEM ETON
JJJ-41-5 DIAZ!NON
62-73-7 DlCI\LORYOS
<,0-51-5 OJMETIIOATE
293-04-4 DISULFOTON
2497-06-5 DISULFOTON .SULFONE
2497-07-6 DISULfOTON suu=O,\IDE
2104-6-l-5 El'N
5(,J.]2-2 ET!llOi\'
1 3194-48-4 ETHOPROP
!5972-W-8
834-12-8
19!2-24-9
3 ! 4-40-9
23184-66-9
200S-41-5
52.34-68-5
101-2!-)
1134-23-2
2921-88-2
333-41-5
. 957-51-7
759-94-4
22224-91-6
51235-04-2
5 l 218-45-2
ALACl!LOR
AMETRYN
ATRAZINE
BROMAC!L
BUTACHLOR
BUn'LATE
Cr\RBOXIN
CI\LORPROl'l!AM
CYCLOATE
CI-ILORPYRH'OS
D!AZINON
DIP!IENAMID
EPTC (EPTAM)
rENAMIPl!OS
J\EXAZINONE
METOLAC!ILOR
TOL-Target Ouantitation Limit-Subject to
change due to instrument sensitivity
T-Tentatively Identified, not confirmed
E-Estimated Value
1.0 u
I.I u
2.5 u
2.5 u
0.8 u
2.1 u
3.5 u
1.0 u
2.3 u
NE u
4.0 u
1.3 u
2.0 u
3.4 N
I.I .N
0.8 N
3.4 N
4.8 N
2.2 N
6.5 N
4.2 N
2.4 N
1.0 N
0.5 N
2.8 N
2.3 N
1.2 N
5.7 N
4.2 N
55-38-9 FENT/I ION 2.U
115-90-2 FENSULFOTIIION 10.0
150-50-5 Fot.EX 2.U
692J-22-4 MEVINP!lOS 1.9
300-76-5 MONOCROTOPHOS 10.0
56-38-2 NALED 4.0
298-00-0 ETHYL PARATIIION 0. 7
298-02-2 METIIYL PARATHION 1.5
299-84-3 l'l\ORATE 15
3689-24-5 RONN EL 0.R
1)1171-74-9 SULr:DTEPP O_J
7786-J-1-7 TEIH\Ur:DS I.I
UNIDENTIFIED PEAKS DETECTED
21087-M-9 METRIBUZIN 1.6
! IJ-48-4 MGK 264 '7
2212-67-1 MOLINA TE 2.1
15299-99-7. NAPROPAMIDE 2.6
27314-1)-2 NORrLURAZON 7. I
1114-7\-2 l'EBULATE (,. 7
!0IU-18-0 l'ROME'IUN 1.)
7287-19-6 l'ROMETRYN 2A
23950-58-5 l'RONAMIDE 7.6
I 39-40-2 l'ROPAZINE 1.0
122-34-9 SIMAZ!NE I.I
1014-70-6 SIMETRYN 2.2
),1014-18-1 TEBUTIIIURON J. l
5902-51-2 TERBACIL 4.4
886-50-0 "J"ERBUTRYN IA
1929-77-7 VERNOLATE 0.6
UNDIENTIFIED PEAKS DETECTED
N-Smnple not analyzed for this compound
D-Detected below quantitation limit
NE-No established TOL
u-Samples analyzed for this cornpound hul not detected
GG16'18
Ug!L
u
u
II
u
l/
l/
u
lJ
u
II
II
II
0
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
COMMENTS:--------------------------------------------------
COUNTY
QU,\D NO
Ill EDELL
REPORT TO 0,,010H00~cc-------Resional Office
COLLECTOR(S) · 0D~.\~l~\\~,c~.,0· ~------
DATE· 7n_q196
Tl/\tE·
PURPOSE·
LABORATORY ANALYSIS
noo 310
COD lligh )40
COD low J35
Coliform: MF Fecal J 1616
Colifo1m: MF To1al J 151).l
TOC
Turbitity
Rnitluc. Suspemkd 530
To1al Suspended solids
pl!
,\l\..alinity to pll 4 5
,\!\..alinil_v 10 p!l S J
C"arbonatc
llica,bor>atc
("a,t,on dio~idc
Ch1<;,1idc
Chromium lk~ IOJ2
Color: True SO
Cyanide 7:0
mg/Kg
mg/Kg
mg]Kg
mg_l'),.:g
i'-1"1 u
m:,;/Kg
n,glK;:
,mib
rng/Kg
mg/Kg
mg/Kg
"'!1.iKg
rngl!-:g
mglKg
u;:{Kg
c.u
mglKg
(h,ncr:
Location or Sile:
IJcKciption of sampling point
S:im1>li11g McthoJ:
1lcma1\..5·
Diss. Solids 70)00
Fluoride 95 I
I la1dncn: to1a! 900
1 lardncss: {non-c.11b) 902
Phc,10ls )2730
Spccir.c Cond. 95
Sulfole
Sulr.dc 745
MUAS
Oil and Grca~
Silica
noron
Nil,\ ;rs N (,IQ
TKN as N 625
NO.'.! •NOJ ,,s n 630
r: Tola! 3s P 665
ro,
Dl\'ISION OF ENVIH.ONi\IENTAL i\lANAGEi\lENT
SA.hlf.LE PRIORITY
□ROUTINE
(D CHAIN OF CUSTODY
@J SAMPLE TYPE
LAMHF:lnll CONSL
mg/Kg
msfKg
mg/Kg
mg/Kg
ug/Kg
uMho5/'cm2
ug!Kg
rn_g.{Kg
mg/Kg
mg/Kg
ms/Kg
mg/Kg
m¥,IK.5
mg/K.11.
mg/Kg
mg/Kg
0E.\1ERGENCY
□
Ag-S1hc1 46566
Al-Aluminum 46557
As-A1scnic 465S I
u~-lhriun1 46558
(3-Calcium 46552
X Cd-Cadium 46559
C1-Chromiun1 46560
C"u·Cop11er IOU
fc-hnn 10-15
X Hg-Mercury "11900
K-ro1a,~ium -16555
Mg-/\!agnciium 917
Mn-Maugancsc 1055
Na-Sodium 929
Ni-Nicl.,cl
X Pb-Lca<l 4656~
Sc-Selenium
7,n z;nc 46567
u;;/Kg
ug/Kg
UJ')Kg
u[I/Kg
u:,lt-:g
1.8 ug/K!!
ug/Kg
ug)Kg
Uf!/K!'-
0 02 ug)K~
ug1K;i,
u~Kg
ug/Kg
"!;/Kg
"!'.IK!'-
18 ug'Kg
ug/K-5
"!:!Kg
L.~b Number
ll:i1e Recei-eJ
111111: Rccci,c:J
Rece"eJ lh·
Nitrogen rn1ieidn
,\cid llcrhiclde,
<,Gl(,2-t
7/J0l'l6
9.50
I).',
GROUNDWATER FIELD/LAB FORM
County It'.'.: e ds Ll
A 11 t::.tv-r1 u /\J
;:J',An,,.U r-,A l{ LC,CJ N
North Caroll no
Department of Environment, Health, end Naturol Resources
DIVISION OF ENVIRONMENTAL MANAGEMENT-GROUNDWATER SECTION
Lab Number ~ t~-~L-
Quad No L (., 7 5 Serial No. _____ _
Lat. 35-, YY' /5 •;v Long. eCJ 0 S"i? / 10 '•u
SAMPLE PRIORITY
@ROUTINE ~ERGENCY 0
Report To: ARO, FRO@, ARO, WaRO, WiRO, f21.cHAIN O CUSTODY
WSRO, Kinston FO, Feo. Trust, Central Off., Other: ·
DateRecei~ 4f?bl tkrrmeq,72()
Rec'd by: u5 From: Bus6 Hand Del.,
Other: ________________ _
Data Entry By: ______ Ck: ______ _
Date Reported: _____________ _
Shipped by: Bus, COIJlie( and Del., Other· ____ ___,,C,,.,M'--'-""~IUN'-"--,,.,Q ~ur~sV.ST . Y
Collector(s): ,., Date ?0'lf'?-l Time /j : c:ru Baseline,~,
FIELD ANALYSES 1 r owner L ,-,,, I l
liance _LUST, Pesticide Study, Federal Trust, Other: ______ _
c11cl• Qno) -
I•.
pH,00 _____ Spec. Cond.94 ______ at 25° C
Temp.10 °c Odor ______ _
Appearance _____ ~----------
Field Analysis By: ____________ _
LABORATORY ANALYSES
BOD. 310 mnil Diss. Solids 70300 mnll Aa • Silver 4G56G uail Organochlorine Pesticides --
COD High 340 mg/I Flouride 951 mrnl Al -Aluminum 46557 uqJI Organophosphorus Pesticides
COD Low335 mail Hardness: Total 900 m~I As -_Arsenic 46551 ugtl Nitroqen Pesticides
Coliform: MF Fecal 31616 1100ml Hardness fnon-carb) 902 mn/1 Ba -8:uium 46558 unil
Coliform: MF Total 31504 1100ml Phenols 32730 u~I Ca -Calcium 46552 mn/1 Acid Herbicides
TOC 680 mail Snecific Cond. 95 uMhos/cm2 --->< Cd -Cadmium 46559 unil
Turbidity 76 NTU Sulfate 945 mnll Cr -Chromium 46560 unil Semivolatile Organics
Residue., Suspended 530 mg/I Sulfide 745 mrul Cu -Co□□er 46562 uail
Fe -Iron 46563 uail
>< Hg -Mercury 71900 uoil Volatile Organics (VOA boitle)
pH 403 unit: K -Potassium 46555 moil
Alkalinity to pH 4.5 410 mg/I Mq -Maqnesium 46554 mail TPH -Gasoline Range
Alkalinity to pH 8.3 415 mg/I Mn -Manaanese 46565 uail TPH -BTEX Gasoline flange
Carbonate 445 mg/I NH_ as N 610 mn,I Na • Sodium 46556 mail
BicmbOnate 440 mnn I TKI\I .. 1\1 "25 mg/I Ni -Nickel unil
Carbon dioxide 405 mq/1 NO + NO as N 630 mn,I I>< Pb -Lead 46564 un/1
Chloride 940 mg/I P: Total as P 665 mrnl Se• Selenium unil
Chromium: Hex 1032 uail Zn· Zinc 46567 uail
Color: True 80 Pt-Co
Cyanide 720 mg/I
Lab Comments:---------------------------------------------------------
GW;54 REV. f'"\
-._.
For Dissolved Analysis -submit filtered sample and write "DIS" in blorlt
cou;,,.'TY
QUAD ;-..:O:
REPORT TO
COLLECTORtS)
Dt\JE·
0,,01_1<0O~~-------RcgiouJI Offi..:e
ll,\111.EN
7/U/96
111>1E
l'URl'OSE
LABORATORY ANALYSIS
BOD 310
COD Hi!'h J-t0
COD low J35
' Colifoon: "\F Fecal Jl61t, < I
' Coliform· 1'.IF Total .11 SO-I ' F
roe
Turbi1i1y
Residue • Su~pcn,kd 5.10
fotJ\ Suspended solids
I'll
.\\lalinitv tu rll ~ S
Albli11iw Ill rl IS .1
Carbon~1c
BicarbO!lJ!t
Carbon di11,idc
[hloridc
Chromi11nl' He, 10.1~
Color· True SO
C, anidc 7:0
rneJL
mg.IL
mglL
1100ml
/1001111
m~,1
NlU
m,:11.
111sll.
unils
m,.:IL
m;;I\.
ms'L
ms'L
ms/L
m_,:11.
u,.:d.
"'
"'~'L
O\\<1cr:
Location Of Si1e:
Ocscriptioo of sampling point
Sarnpling Method:
KcrnJ,~s
Diss Solids 70JOO
flumide 951
I l~rdncs,. ll!tJI 900
I !a,dness: (non-carb) 902
l'hcnols 31730
Specific Cond. 95
Sulfate
S1ilr,de 745
1'.11JAS
Oil ;,.n,.! G,casc
s,r;ca
Bnmo
NIO as N 610
TJ..:N as N 625
' NO2 •NO3 a, n 630
I': To1al :1s I' 665
1'04
I
DIVISION OF ENVlllON1\IENTAL i\lANAGEI\IENT
SAl-11'LE PRIORITY
[DROU'l'INE
ID C!l,\INOFCUS·1ODY
0 S,\Ml'LE TYl'E
ltOl)NEY HII0\"1111,1. \\'ELI.
mg_lL
rnglL
n1glL
m_,:IL
ug,11.
uMhoslcm2
mglL
rug.IL
mHJl.
m!(.IL
mg.IL
0.02 mg_lL
"'-""'L
0.53 m;;IL
m;;IL
n1glL
□
,\g·Sihc< 46566
,\I-Aluminum 46557
As-Arsenic 46551
lfa-lJ~rium 46558
C3·Cakium 46552
Cd·Cadium 46559
Cr·Chromium 46560
Cu• Coppc1 J0-12
Fe· hon 10·1S
' Ilg-r,.tc,cury 71900
K-Potassi,11n 46555
/II~-Ma;;ncsium 927
r,.1n.:,.iangancse 1055
Na-Sodium 929
Ni-Ni,~d
l'IJ-Lc;,.d 46564
Sc·Sclc1>ium
Zn Zinc 46567
CO:-,\;\IE~"IS: ~-J ll.u-:, !'OM ~ f\ L I nr, ,vy-, ", D\ 0 (\O -n
I, I, .
-
ug,11.
u~l.
U!_t./L
u~L
mg,11.
ug.r\.
ug,11.
ugJL
Ug/!.
<0.2 ugll. ·'
Ulf;I\.
rng,11.
u;;•l.
mgl!.
ug.il.
uglL
"S'I.
"!'-'I.
I.al, Nurnl..,, <i<; I 5H5
Ihle Re~ci,c,I 111!-/?(,
·r unc Recci, cd ? 1 S ,\1-1
Rccci,cd ll)· DS
11.clcascJ B} IJS
Hale •q><>rtcJ : 960826
O,g~nochlorinc Pesticide, ~
O,g.,.,,orhusphorus Pesucidc,
,_. c-,
Nitro~cn l'n11cidc, f',)
,aJ
Acid llc,bicidc,
"
"
Scmi,olat,lcs •·
l l'l l•ll1csd Ran!_!<'
\'111,,t,lc (hi,:,,,.in (\"(),\ hon!c)
I Pl 1-liasolinc 11.ansc
I rll-111 EX Cia10linc Ran;;c
l
: ,,,
GROUNDWATER FIELD/LAB FORM
BOD. 310 mnll
COO High 340 mg/I
COD Law 335 mall
-~ Coliform: MF Fecal 31616 1100ml
I'-./ Coliform: MF Tolal 31504 /100ml
TOG 680 mail
Turbidity 76 NTU
Residue., Suspended 530 mg/I
pH 403 unit:
Alkalinity to pH 4.5 410 mg/I
Alkalinity to pH 8.3 415 mg/I
Carbonate 445 mgil
BicorbOnate 440 mc;I
Carbon dioxide 405 mc;I
Chloride 940 mg/I
Chromium: Hex 1032 uc;I
Color: True 80 Pt-Co
Cyanide 720 mgil
1--x
SAMPLE PRIORITY
52!ROUTINE · □EMERGENCY
~!ZJcHAIN OF CUSTODY_
I .
Diss. Solids 70300 mnll
Flouride 951 mnll
Hardness: Total 900 m0 'I
Hardness (non-carb\ 902 moll
Phenols 32730 uon
Snecific Cond. 95 uMhos/cm2
Sulfate 945 m0 •t
Sulfide 745 mnll
:........,.,,
NH as N 610 mnll
I TKN --P...I ,.,..,. mg/[_
NO +NO as N 630 moll
P: Total as P 665 mall
.-North Caroline
Department of Environment, Health, and Natural Resources
· F ENVIRONMENTAL MANAGEMENT· GROUNDWATER SECTION
0 Date Rece,r· ,...,..-,4,c,.""-1µ-"'-
Rec'd by:-'t..Lc~'---rom: us ouner, and Del.,
Other: ________________ _
Data Entry By: ______ Ck: ______ _
Date Reported: _____________ _
Ao • Silver 46566 unll Oraanochlorine Pesticides -
Al -Aluminum 46557 u □II Organophosphorus Pesticides
As • Arsenic 46551 uall Nitroaen Pesticides
Ba -Barium 46558 ua/I
Ca -Calcium 46552 mn/1 Acid Herbicides
Cd• Cadmium 46559 uall
Cr -Chromium 46560 ua/I Semivolatile Organics
Cu -Conner 46562 uall
Fe -Iron 46563 uall
Hq -Mercury 71900 ugil I-,.,< Volatile Organics (VOA ballle)
K -Potassium 46555 ma/I
Ma -Maanesium 46554 mQ/I TPH • Gasoline Range
Mn -Manqanese 46565 uall TPH · BTEX Gasoline Range
Na -Sodium 46556 mal
Ni -Nickel U0 'I
Pb -Lead 46564 uall I
Se• Selenium uall \ I
Zn -Zinc 46567 unll
Lab Comments: _____________________________________________________ _
GW-54 REV. 6'9-i For Dissolved Analysis -submit filtered sample and write "DIS" in block.
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
75-35.4
75-09·2
156·60-5
75-34-3
590·20-7
156-59-4
67-66-3
74.97.5
71-55·6
563-58-6
s·G-23·5
107-06·2
79•01·6
78-87·5
75-27-4
74-95-3
10061-01-5
10061-02·6
79-00·5
127-18-4
142-28-9
124•48-1
106.93.4
108-90-7
630-20-6
75-25-2
79-34-5
T □L·
T-
E·
U·
N-
0-
M·
COMMENTS:
WATER
1. 1-Dichloroethene 0.75
Methylene Chloride 10
trans-1, 2•Dichloroethene 0.75
1, 1 ·Dichloroethane 0.25
2, 2 · Dichloropropanc 0.25
cis-1,2•Dichlorot?thene 0.25
Chloroform 0.25
Bro moc hi or ome thane 0.75
1, 1, 1-Trichloroethane 0.25
1, 1 ·Dich!oropropene 0.25
Carbon Tetrachloride 0.75
1,2-0ichloroethanc 0.25
Trichloroethene 0.25
1,2·Dichloropropane 0.25
Br ornod ich1or o rne I h ane 0.25
Oibromornetl1ane
cis-1,3-Dichloropropenc 0.25
tr ans-1,3•Dich!oropropene 0.25
1, 1,2-Trichloroethane 0.25
Tetrachloroethene 0.25
1,3-Dichtoropropone 0.25
Dibromochloromethane 0.75
1, 2-0ibromoethane 1
Chlorobenzene 0.25
1, 1, 1,2-Tetrachloroethane 0.25
Bromoform 0.5
1, 1,2,2-Tetrachloroethane 0.75
Target Quantit.ition Limil• Subject to
change due to instrument sensitivity
Tentatively Identified, not confirmed
Esti111ated Value
Samples analyzed for this compound but not detected
Sample not analyzed for this compound
Detected below quamitation limit
GC/MS Analysis performed
EHNA/DEM LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 96-18-4 1, 2,3-Trichloropropane
u 108-86-1 Bromobenzene
u 95-49-8 2·Ch1orotoluene
u 106-43-4 4·Chlorotoluene
u 541-73-1 1 ,3-Dichlorobcnzene
u 106·46· 7 1.4-Dichlorobenzene
u 95-50·1 1,2-Dich!orobenzene
u 96-12·8 1, 2-Dibromo-3-Chloropropane
u 120-82-1 1,2,4-Trichlo1obenzcne
u 87-68-3 Hexachlorobutadiene
u 87-61-6 1,2,3-Trichlorobenzene
u 1634·04-4 Mcthyl-tert-butyl ether
u 71-43-2 Benzene
u 108·88·3 Toluene
u 100·41·4 Ethyl benzene
u 108-38-3 m,p·Xylenes
u 95-4 7-6 a-Xylene
u 100-42-5 Styrene
u 98-82-8 lsopropylbenzcnc
u 103-65-1 n-Propylbenzene
u 108-67-8 1,3,5-Trimethylbenzene
u 98-06·6 tert-Butylbenzene
u 95-63-6 1,2,4-Trimethylbcnzene
u 135-98-8 sec·Butylbenzcne
u 99-87-6 p•isopropyltoluene
u 104-51·8 n-Butylbenzene
u 91-20-3 Naphthalene
Gasoline Range Estimated Total Pelrolcurn Hydrocarbon
Other purgeables detected
(up lo 10 highest peaks)
NO VOLATILE ORGANIC COMPOUNDS
DETECTED BY GC/ELCD/PID.
LAB NO. GG 1585
SUPEHVISOA r-;;:ek·,
DATE&'.1.9
HHEnEO BY ~ .
DAIE
0.25 u
u
0.25 u
0.25 u
0.25 u
0.25 u
0.25 u
1 u
0.25 u
0.25 u
0. 75 lJ
5 u
u
u
1 u
' u
u
u
u
u
u
u
u
u
u
u
u
mg/L rng/L
0.25 IJ
Detected
ug/L
=JUNTY
UAD NO:
!REDELL
IOf'ORT TO _,,_l_ll_O _________ Rcgional Office
< ILLECTOR(S): FINLE,. \ r E --''--'c,,",a,,c,-------
1 \IE·
'!Rl'OSE·
.AIJORATORY ANALYSIS
llOOJ10 mg1L
COD lligh J40 mg/L
COD Low JJS rng/L
Coliform: MF fecal JJ6J6 /IOOrnl
Coliform: r-.lFl'olalJJSQ.1 /IOOml
roe mg/I
Turbitity NTU
Residue., Suspended 5JO mg/L
Total Suspended solids mg/L
pH unils
,\lblinity to pl I 4. S mglL
,\lkalinit_v w pl I 8.J rnglL
\arbona1c mglL
llicarbon:i!c mglL
Carbon dio,idc-mg/L
Chloride mg1L
Chrormum He, 1032 uglL
Color; Tiu,:, 80 '" C,ranidc 720 rnglL
Owner;
Localion 01,Si!c
Dcscrip1ion of sampling p(lint
Sampling Method
Remar~s
Diss. Solids 70300
Fluoride 951
lla,dm:ss: total 900
I la1dncss: (non-c:irb) 902
Phenols J27JO
Specific Cond. 95
Sulfate
Sulfide 745
MUAS
Oil and Gre;l',C
Silica
Jlomn
NJIJ asN610
IKNasN625
-' N02 1NOJasn6JO
I': Tola! as r 665
1'0-l
IH\'1S101~' OF £NVIHON1\IENTAL 1\UNAGEMENT
SM,1PLE PRIORITY
E)ROUTJNE
~ Cllt\lNOFCUSl'ODY
El S,\Ml'LE TYl'E
O1:MERGENCY
□ IH)IIE/rlSo,-.,· UENTAL TH,\ILEH l'OT"IS nJ,:S.
mg/L Ag-Sihcr 46566
mg/L Al·Aluminum 46557
mg,'L As-Arsenic 46551
1ng/L Ba-Barium 46558
ug/L Ca·Calciurn 46552
u,~lhos/cm2 Cd-Cadium 46559
mg/L Cr-Chromium 46560
mg/L Cu-Copper 1042
mg.IL Fe-lro11 10-15
rng/L -' Hg-Mcrcur)' 71900
mg/I. J..,:.Polassium 4<,555
Mg-Ma!,':11e.siu111 927
Mn-Manganese 1055
0.01 mg/L Na-Sodium '129
0,1 mg/L Ni-Nid,d
1,8 mgd. Pb-Lead -ll>St,-l
mg/I. Sc-Selenium
mglL Za -Zinc•l6SC.7
ug/1.
•s'L
,wL
ug/L
mg/L
,wL
,wL
ug/L
,wL
<0.2 ugtL -'
mglL
mtVL
ug/L
mg/L
ug/L
ug/L
ug/L
ugll.
Lab Number GGl40S
Dale Recci,ed 7/2196
Time Recci,cd
Rccci,ed By
Orga,1ochloriue Pesticides
Org:mophosphorus Pesticides
Nioogen Pesticid,:,s
Acid Herbicides
Serni,·ol:itiles
Tl'II-D"rcsd Range
9:20AM
us
Volatile Organics (VOA boulc)
l'l'H•Gasoli11e Range
l'l'll•llTEX G:isoline Range
6GUC5 JUl
GROUNDWATER FIELD/LAB FORM
Field Analysis By: ~~ Remarks ~L-, .,Ca<-/ 7 if" L j LABORATORY A~ALYSES -,,..,
BOD. 310 mall Diss. Solids 70300 mall COD High 340 mg!/ Flouride 951 mnn COD Low335 mall Hardness: Total 900 mg/I Co/ilorm: MF Fecal 31616 1100ml Hardness tnon-carbl 902 mail Co/ilorm: MF Total 31504 /100ml Phenols 32730 uall TOG 680 mg!/ Sgecific Cond. 95 uMhos/cm2 Turbidity 76 NTU Sulfate 945 mall I Residue., Suspended 530 mg/I Sulfide 745 mall
.,,.-pH 403 unit~
Alkalinity to pH 4.5 410 mg/I
Alkalinity to pH 8.3 415 mg!/
Carbonate 445 mg/I NH as N 610 mail Bicarbonate 440 mnlj TKl\l ... ~ N ,,,,.,r: mgll Carbon dioxide 405 mg/I £.. NO +NO as N 630 mg!I Chloride 940 mg/I P: Total as P 665 mall Chromium: Hex 1032 u[J/I
Color: True 80 Pt-Co
Cyanide 720 mg!/
Lab Commenls:
North Carolina
Department of Environment, Hcallh, and Natural Resources DIVISION OF ENVIRONMENTAL MANAGEMENT. GROUNDWATER SECTION
-5' U!Jlp, .a1 r," _ _ p .......,..,...., ~----·z...,.. ~ I {pUmplllQ tfne, .air II~. '"")-:;,..__/ A,,,__,,,!> ~ ,,--_,,, 6._e,.. -~
Ao • Silver 46566 uall Organochlorine Pesticides
Al -Aluminum 46557 uall Organophosphorus Pesticides As • Arsenic 46551 ua/I Nitroaen Pesticides
Ba -Barium 46558 uall
Ca -Calcium 46552 • mall Acid Herbicides
Cd -Cadmium 46559 uall
Cr -Chromium 46560 uall Semivolatile Organics
Cu -Coooer 46562 u[J/1
Fe -Iron 46563 uq/I
Hg -Mercurl'. 71900 u9!I x-Volatile Organics (VOA bottle) K -Potassium 46555 mall
Mq -Maqnesium 46554 mqil TPH -Gasoline Range
Mn -Manqanese 46565 U(JII TPH -BTEX Gasoline Range Na -Sodium 46556 mall f Ni -Nickel ug/1 ' I
Pb -Lead 46564 uall \ I Se -Selenium uall \J Zn -Zinc 46567 uall .
.
----------------------------------------------------------
GW-54 REV.' For Dissolved Analysis -submit filtered sample and wrile "DIS" in bloc~.
Ri!POATED BY
CHECKED BY
REVIEWED BY
SAMP~E TYPE:
75-35-4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79-34-5
TOL-
T-
E·
U-
N-
D·
M-
COMMENTS:
WATER
1, 1-Dichloroethene 0.75
Methylene Chloride 10
trans-1,2-Dichloroethene 0.75
1, 1-Dichloroethane 0.25
2, 2-Dichloropropane 0.25
cis-1 ,2-Dichloroethene 0.25
Chloroform 0.25
Bromochloromethane 0.75
1, 1, 1-Trichloroettiane 0.25
1, 1-Dichloropropene 0.25
Carbon Tetrachloride 0.75
1 ,2-Dichloroethane 0.25
Trichloroethenc 0.25
1,2-Dichloropropane 0.25
Bromodichloromethane 0.25
Dibromon1ethane 1
cis-1,3-Dichloropropene 0.25
trans-1,3-Dich!oropropene 0.25
1, 1,2-Trichloroethane 0.25
Tetrachloroethene 0.25
1,3-0ichloropropane 0.25
Dibromochloromethane 0.75
1,2-Dibromoethane 1
Chlorobenzene 0.25
1, 1, 1,2· Tetrachloroethane 0.25
Bromoform 0.5
1, 1,2,2-Tetrachloroethane 0.75
Target Ouantitation Limit-Subject to
change due to instrument sensitivity
Tentatively Identified, not confirmed
Estimated Value
Samples analyzed for this compound but not detected
Sample not analyzed for this compound
Detected below quantitation limit
GC/MS Analysis performed
IJINll/1.lEM 1./\11(111/\ I UltY
VOLATILE ANAL YT !CAL REPOH f
ANALYSIS AESUL TS
u 96-18-4 1,2,3-Trichloropropane
u 108-86-1 Bromobenzene
u 95-49-8 2-Chlorotoluene
u 106-43-4 4-Chlorotoluene
u 541-73-1 1 ,3-Dichlorobenzene
u 106-46-7 1,4-0ichlorobenzene
D 95-50-1 1,2-Dichlorobenzene
u 96-12-8 1,2-0ibromo-3-Chloropropane
u 120-82-1 1, 2,4-Trichlorobenzene u 87-68-3 Hexachlorobutadicne
u 87-61-6 1,2,3-Trichlorobenzene u 1634-04-4 Methyl-tert-butyl ether u 71-43-2 Benzene
u 108-88-3 Toluene
u 100-41-4 Ethyl benzene
u 108-38-3 m,p-Xylenes u 95-47-6 a-Xylene
u 100-42-5 Styrene
u 98-82-8 lsopropylbenzene
u 103-65-1 n-Propy/benzene
u 108-67-8 1,3,5-Trimethylbenzene
u 98-06-6 tert-Butylbenzene
u 95-63-6 1,2,4-Trimethylbenzene
u 135-98-8 sec-Butylbenzene
u 99-87-6 p-isopropyltoluene
u 104-51-8 n-Butylbenzene
u 91-20-3 Naphthalene
Gasoline Range Estimated Total Petr61eurn Hydrocarbon
Other purgeables detected
(up to 10 highest peaks)
NO VOLATILE ORGANIC COMPOUNDS DETECTED BY
GC/PID.
I /\II NII, nn Jitllli
0.25 u
u
0.25 u
0.25 u
0.25 u
0.25 u
0.25 u
u
0.25 u
0.25 u
0.75 u
5 u
u
u
1 u
2 U,
u
u
u
u
u
u
u
u
u
u
u
mg/l mg/l
0.25 N
Detected
ug/L
1>UNTY
U,\DNO.
95 AUG 12 P11 3: 03
IHEDELL
EPORTTO
IJLLECTOR(S)
.\TE:
-:-:-~c:cEc\-. ________ Rq:i,:,na\ O!licc
711/96
l,\\E·
IJRPOSE·
.AllORATORY ANALYSIS
800)10
COD Hi;h JJO
COD L{>W .1)5
Colifonn: ~lF Fcc:;,.l 31616
Coliform Ml'Tota1Jl50.\
TQC
Turbi1i1y
Residue . Su~pcndcJ 5~0
T oial Suspended S<lhds
pl\
Allalinity to p/1 .\ 5
All.::P.lmilv lo pl\ 8.J
Cart>on:itc
llica,bonalc
CaiOOn J,o,idc
Chloride
Chiomiurn; lk:-. 103~
Colo,: TruC' 80
C.,·anidC' 7.'.!0
O:\IMENTS:
m.!:_11.
mg.il
mg.IL
1100ml
flOOml
mg/I
NTU
m;:.11.
m_,;/1.
lHlll~
mi:,'l.
m;t·'L
111;,II.
mg.IL
mgll.
m~.IL
U!!'L
'"
11,g'L
O"ucr:
location or Site
Dcsc1ip1ion of =plini; point
Sampling Method·
Rcm3il,$·
Dis~ Solids 70JOO
Fluo1idC' 'lS l
lb1Jness· total 900
l l;,.rJnen-(non-c;i.rb) 902
l'hcno\s 327J0
Specific Cond. 95
Sulfote
Sulfide 745
1'1BAS
0,1 and Grease
Si lie;,.
Boron
NIIJ as N 610
fKN ;i.s N 625
' NO2 +NOJ as n 630
I': T 01al as r 665
ro.1
DIVISION OF ENVlllONI\IENTAL I\IANAGE;\IENT
.SAM!:l,_E rRIORITY
[]1t0UllNE
[] CIIAINOf'CUSTODY
EJ St\MPLE TYPE
Ai.LEN C,\SCAIHlAN
rn!!IL
mg/L
m!!IL
rng/L
u!!IL
u1'1hos/cm2
mg/L
mp)L
mg.IL
mg/L
mg/L
0.01 mglL
0.2 mg/L
\1 n1g/L
1n1;IL
n,l!,L
□EMERGENCY
□
Ag-Sih er 46566
Al-Aluminum 46557
As-Arsenic 46551
Ila-Barium 46558
Ca•Calcium 46551
Cd-radium 46559
Cr•Chrumium 46560
Cu-Cuppcr 10~2
re-hon 1045
' 11.,:-Mercury 71900
K-Potanium ~6555
Mg· 1'1agne~ium 927
Mn-Manganese IOSS
Na• So<lium 919
Ni-Nickel
l'b·l.CJd 4(,564
Sc·Sdcnium
Zn _zinc 46567
Lah Nurnb<:r 6(;) -'IJ-'
UJtc Recci,cd · 1/1196
luncRccei,cJ· 9:>0A,',.J
Rccei>td lly !JS
"s'L Chsanochlor,nc Pntic,Jts
u!UI. (ltf.knophosphorus Pc11iciJcs
ug/L N11to11cn Pn1icides
"i;'L
mg/l Ac,J lkrbiciJn
ug/L
"i;'L Scrni,ub111n
"s'L l 1'11-Dind R;,.n_.:e
"s'L
0.9 ugll ' \'obtilt Or~anin (\"0,\ hunk)
rn_o/L
mg/I. l l'IHiawlinc Ran~e
U!,!IL I f'I HI I I::\ (ia1olmc lbnl.'.e
rn!_r:IL
up)L
u)til.
u.:'L
U!1/L
6G1<1).< JUI.
GROUNDWATER FIELD/LAB FORM
County ~,,-,dL(I
Quad No Lt:-7 n 7 Serial No.______ SAMPLE PRIORITY
._;, o o" 5Z! '/,/ ,,
Lat. 3 "> rz.". S-d ,, Long.~"--~~!'_ ___ ~UTINE □EMERGENCY
[£}tHAIN OF CUSTODY
Report To: ARO, FRO~RO, WaRO, WiRO,
WSRO, Kinston FO, Fed. Trust, Central Off., Other: ________ _
·th Carolina
Department of ~
DIVISION OF ENVIRONl.s
,·1ment, Health, end Natural Rosources
<',L MANAGEMENT. GROUNDWATER SECTION
0
Lab Number -~f;!,;?{,t-,'--""'~e-=-:-=-:-s---
~""'--'-~,<.L..Time Cj ·. d, U____
-"-61=""--From: Bus~ Hand Del.,
Other: _______________ _
Data Entry By: ______ Ck: ______ _
Date Reported: _____________ _
Shipped by: Bus~r. Hand Del., Other_·------------=--
i"'° I whrn Mon, +,,,·,,y
31" Purpose: o
Collector(s): 2-:-z '9-,._, Date 7 /1 / 1 &,. Time /2--,,,~ Baseline, Complainl, Compliance LUST Pesl1cide Sludy, Federal Trust, Other: J>:: 3 J./ 2..2.. :r~c •
~ ·--Jc.-cle OOII)' ~
FIELD ANALYSES Owner s,::.,,,__/.d,
pH400 t-.O Spec.Cond.9, -~7~·=o~at25°C 3~7 ( £d.'-'r<L,-, / r,,,,,_ 5-;rr-...r>..csv,//.,_
Temp.10 2 f,' 0 c Odor _______ Description of sampling point -""'~2f?>-:1F~-e-±_~a..._+_~b~"--d,_<_P_..f_~-ir_a.,~/-~~------------
Appearance c..c~ ~~ Sampling Method p......,..__,, Sample Interval _______ _
?,,7q..,.____.g R -....,.~,, -~~, ..... ,.,,c) b L ~
Field Analysis By: . < ')' emarks v2:J,M'
~ .... ....,...-p ~ .,..
I ~l_z£J::,,_ (pu~lflO llm.!4 I•~;) ,
I ABORATGnY ANAi YSES 5, ,,, ,I 01,. J ,-..,
BOD. 310 mn/1 Diss. Solids 70300 mnll Ag • Silver 46566 uQII Organochlorine Pesticides
COD High 340 mg/I Flouride 951 mnl1 Al • Aluminum 46557 UQII Organophosphorus Pesticides
COD Low 335 mall -Hardness: Tolal 900 moil As -Arsenic 46551 uoil Nitroqen Pesticides
Colilorm: MF Fecal 31616 /100ml Hardness (non-carb\ 902 ma/I Ba -Barium 46558 unn
Coliform: MF Tolal 31504 /100ml Dhnnols 32730 urol Ca -Calcium 46552 moil Acid Herbicides
TOG 680 mQII Soecilic Cond. 95 uMhos/cm2 Cd • Cadmium 46559 uo/I
Turbidily 76 NTU Sulfate 945 moil Cr -Chromium 46560 unA Semivo1atile Organics
Residue., Suspended 530 mg/I Sulfide 745 moil Cu -Conner 46562 unl1
Fe -Iron 46563 uo/I
y Hg• Mercury 71900 uq/I \..., Volatile Organics (VOA bottle)
pH 403 units ' K -Potassium 46555 mg/I '
Alkalinily lo pH 4.5 410 mg/I Ma -Maanesium 46554 mQ/I TPH • Gasoline Range
Alkalinily lo pH 8.3 415 mg/I Mn • Manqanese 46565 uQII TPH . BTEX Gasoline Range
Carbonate 445 mg/I NH, as N 610 mQ/I Na • Sodium 46556 mq/I I
Bicarbonate 440 man I TKN oo N co< mn/1 Ni· Nickel ua/I I
Carbon dioxide 405 ma/I y NO +NO as N 630 mnn Pb . Lead 46564 ua/I ' I
Chloride 940 mg/I P: Tolal as P 665 mail Se -Selenium unn \ I
Chromium: Hex 1032 uq/I Zn -Zinc 46567 unA \I
Color: True ao Pl•Co
'
Cyanide 720 mg/I
Lab Comments: ________________________________________________________
_
GW•54 REV. r For Dissolved Analysis -submit filtered sample and write "DIS" in blod.
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
75.35.4
75-09-2
156-60-5
75.34.3
590-20-7
156-59-4
67-66-3
74.97.5
71-55-6
563·58-6
56-23-5
107-06-2
79·01-G
78-87-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79.34.5
TOL-
T·
E·
U·
N·
D-
M·
COMMENTS:
WATER
1, 1-Dichlorocthcne 0.75
Methylene Chloride 10
trans-1 ,2-Dichloroethene 0.75
1, 1-Dichloroethane 0.25
2, 2-Dichtoropropane 0.25
cis-1 ,2-Dichloroethenc 0.25
Chloroform 0.25
Bromochloromethane 0.75
1, 1, 1-Trichloroethane 0.25
1, 1-Dich!oropropene 0.25
Carbon Tetrachloride 0.75
1,2-Dichloroethane 0.25
Trichloroethcne 0.25
1 ,2-Dichloropropanc 0.25
81 omodichlororncttianc 0.25
Dibrorno1nc1ha11e 1
cis-1,3-Dichloropropene 0.25
trans-1.3-Dichloropropene 0.25
1.1,2-Trichloroethane 0.25
Tetrachloroethene 0.25
1, 3-Dichloropropane 0.25
Di br omochloro me thane 0.75
1,2-Dibromoethane
Chlorobenzene 0.25
1, 1, 1,2-Tetrachloroethane 0.25
Bromoform 0.5
1, 1,2,2-Tetrachloroethane 0.75
large\ Ouantitation Limit• Subject to
change due to· instrument sensitivity
Tentatively Identified, not confirmed
Estimated Value
Samples analyzed for tllis compound but not detected
Sample not analyzed for this compound
Detected below quantitation limit
GC/MS Analysis performed
EHNR/DEM LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 96-18-4 1,2,3-Trichloropropane
u 108-86-1 Bromobenzene
u 95-49-8 2-Ch1orotoluene
1.1 106-43-4 4-Chlorotoluene
u 541-73-1 1,3-Dichlorobenzene
2.6 106-46-7 1 ,4-0ichlorobenzene
u 95-50-1 1 ,2-Dichlorobenzene
u 96·12-8 1 ,2-Dibromo-3-Chloropropane
u 120-82-1 1 ,2,4-Trichlorobenzene
u 87-68-3 Hexachlorobutadiene
u 87-61-6 1, 2, 3-Trichlorobenzene
u 1634-04-4 Methyl-tert-butyl ether
D 71-43-2 Benzene
u 108-88-3 Toluene
u 100-41-4 Ethyl benzene
u 108-38-3 rn,p-Xylenes
u 95-47-6 a-Xylene
u 100-42-5 Styrene
u 98-82-8 lsopropylbenzene
u 103-65-1 n-Propylbenzene
u 108-67-8 1,3,5-Trimethylbenzene
u 98-06-6 tert-Butylbenzene
u 95-63-6 1,2,4-Trimethylbenzene
u 135-98-8 sec-Butylbenzene
u 99-87-6 p-isopropyltoluene
u 104-51-8 n·Butylbenzene
u 91-20-3 Naphthalene
Gasoline Range Estimated Total Petroleum Hydrocarbon
Other purgeables detected
(up to 10 highest peaks)
NO VOLATILE ORGANIC COMPOUNDS
DETECTED BY GC/PID.
LAB NO. 6G1404
DATE 7 j. JR SUPERVISOn ~fj
EtJTEnED BY D5 _
DAlE~
0.25 u
u
0.25 u
0.25 u
0.25 u
0.25 0.25
0.25 u
1 u
0.25 u
0.25 u
0.75 u
5 u
u
u
u
2 u
u
u
u
u
u
u
u
u
u
u
u
mg/l mg/L
0.25 "
Detected
ug/L
"t
COUNTY
QUAD NO:
REPORT TO
COLLECTOR(S)
DATE:
c~c~c~"~cLcEcSc--------Regional Office
5/15/96
TIME:
PURPOSE:
LABORATORY ANALYSIS
BODJ10
COD I ligh 340
COD Low JJS
Coliform: MF fec:il 31616
Colifom1: MF Tota! 31504
TOC
Turbitity
Residue., Suspended SJO
Total Suspended solids
pH
Alkalinity to pl-I 4.5
Alkalinity to p!l 8.3
Carbonalc
Bicarbonate
Carbon dioxide
Chloride
Chromium: I-fox I 03:!
Color: True 80
Cpnide 720
COMMENTS:
mg/L
mg/I,
m&'L
/IOOml
1100ml
m,0
NTU
mg/L
mg/L
units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
,g/L
'"
mg/L
Owner:
Location or Site:
Description of s.impling point
Sampling Method:
Remarks:
!Jiss. Solids 70300
fluoride 95!
I !ardness: total 900
Hardness: (non-carb) 902
Phenols 32730
Specific Cond. 95
Sulfate
Sulfide 745
MBAS
Oil and Grease
Silica
Uoro11
N113asN6IO
TKN as N 625
X N02 +N03 as n 6JO
P: Total as r 665
1'04
Tin!<;.,. r:,_T-:/·:;:c: :·::: ~ e-rv'tc e
.. --~ ... ! :: !-:''.
<::r~ . 1u\1
DIVISION OF ENVIHONi\lENTAL i\lANAGEi\1£NT.
Chemislry L11liornlorJ R,port / Grouml Wattr Quality
SAMPLE PRIORITY
(DROUTJNE
ID C!IAINOFCUSTOOY
E] SAMPLE TYPE
CIIRIS DAVIDSON RESO.
rng/L
mg/L
mg/'L
mg/L
,g/L
uMhos/cm2
mg/L
mg/L
mg/L
mg/L
my'L
mg/L
mg/L
1.6 mg/L
mg/L
mg/L
□EMERGENCY
□
Ag"Silvcr 46566
AI-Aluminu1u 46557
As-Atscnic 46551
Ua-ll:uium 46558
Ca-Calcium 46552
Cd-Cadium 46559
Cr-Chromium 46560
Cu-Copper 1042
l'c-Iron 1045
X Ilg-Mc1cury 71900
K-l'otassium 46555
Mg-Magnesium 927
Mn-Manganese 1055
Na-Sodium 929
Ni•Niekcl
Pb-Lead 46564
Se.Sclcni"m
Z11 Zinc 46567
Lab Number 6G 1070
Date Received : 5/16196
Time Received : 9.00 AM
Received Dy DS
"g/L Organochlo,ine l'csticidcs
ug/L Organophosphorus rcsticidcs
,pJL Nitrogen l'csticidc~
,,tL
mwL Acid lle1bic1dcs
og/L
og/L SemivolaLilcs
,g/L TPII-Diesel Range
,g/L
<0.2 ug/L X Volatile Organics (\'OA bott!eJ
mg/L
mg/L Tl'll-Gasolinc Range
,g!L TPJI-OTEX G;isolinc Range
mg/L
,we
,g!L
o&'L
'"'-
6G10JOUA1
,j . 0.
N•o r I h Caro Ii n a
GROUNDWATER FIELD/LAB FORM ., . _ '. .. , _ ., Qepartment ol Environment, Health, and Natural Resources
~ JiS1i(VJ~9~· OF ENVIRONMENTAL MANAGEMENT. GROUNDWATER SECTION
County Ic<:Ml,
Quad N~~7~h~--Serial No. ______ _
Lat. 55--.,'13101iLrJ Long. f!u 0 571 SZfL/Lv
Report To: ARO. FR~RO. WaRO. WiRO,
SAMPLE PRIORITY
@ROUTINE □EMERGENCY
16jcHAIN OF CUSTODY
WSRO, Kinston FO, Fed. Trust, Central Off .. Other: ________ _
Shipped by: Bus{C~. Hand DeL, Other·--.,----------,~-
0 Other: ________________ _
Data Entry By: ______ Ck: ______ _
Date. Reported: _____________ _
~~ / /_ /J !Y ,,-,, Purpose:
Collector(s): _j)d,._(g.,..,, Date !Ir l ]z'f:C ' Time I J.. : L) Baseline, Complaint, Compliance, LUST, Pesticide Study. Federal Trust, Other:
=l:j / ~1/'~ :-,,. / I 1cuc!eone)
r,. .. ,..,. _;;._, .1'1. J '{ 2. -:,_
/'..{f,, -L'-,. "'"'-.
El ELD AN ALYSE s s-/ r,) Owner _.,,C""/,,'-',-L.L.' lL. _J)c,..l ""-'"'""'"'cJ=-:oc:C,cc'l~<-;--'lR,'e..,;.,:-",""<:!"'~~( OS<..,...,---------------------
pH -<,u Spec. Cond.94 So a~ C Location or site _5=,!{..__,t~c~; ,,,_•,-_,_i~::S~f"':.i;,._....:f~C'-1'!-'"-~"',(~(;,~~---~--,,--,,-----,-----------
Tei'n~.10 L 0 c Odor -· · Description of sampling point. ~-""'-k.1.;,P-,:'/ /4✓{~ 5,;;,k..
Appearance c!..u:..,.-( <·l:-<-.{I Sampling Method J'.2 . Sample Interval _______ _
~;111Q1,11lc)
Field Analysis By: c_ I Remarks---------------======-----------------(pumping time, i.lf\emp. etc.)
LABORATORY ANALYSES
BOD. 310 ma/I Diss. Solids 70300 mn!I Aq -Silver 46566 , uq/1 OrQanochlorine Pesticides
COD High 340 mg/I Flouride 951 ma/I Al -Aluminum 46557 ug,I Organophosphorus Pesticides
COD Low 335 ma/I Hardness: Total 900 mrol I As -Arsenic 46551 ua/1 Nitrogen Pesticides
Colilorm: MF Fecal 31616 /100ml Hardness (non-carb\ 902 ma/I · Ba -Barium 46558 ua/1
Colilorm: MF Total 3 t 504 1100ml Phenols 32730 ua/1 Ca -Calcium 46552 mg.JI Acid Herbicides
TOG 680 ma/I Snecific Cond. 95 uMhos/cm2 Cd -Cadmium 46559 ua/I
Turbidity 76 NTU Sullate 945 mc,/1 Cr -Chromium 46560 ug/1 Semivolatile Organics
Residue., Suspended 530 mg/I Sullide 745 mq/1 Cu -Coooer 46562 ug/1
Fe -Iron 46563 ugtl
Iv Ha -Mercury 71900 ug!I l?'S Volatile Organics (VOA bottle)
pH 403 unit!: K -Potassium 46555 mgtl
Alkalinity to pH 4.5 410 mg/I Mg -Magnesium 46554 mg/I TPH -Gasoline Range
Alkalinity to pH 8.3 415 mg/I ' Mn -Manoanese 46565 UQJI TPH -BTEX Gasoline Range
Carbonate 445 mg/I NH as N 610 mall Na -Sodium 46556 mq/l
Bicarbonate 440 ma/I : TKN -~ N C">C' -"" Ni -Nickel ug/1
Carbon dioxide 405 mq/l --.,, NO, + NO, as N 630 mg/I Pb. Lead 46564 uq/l
Chloride 940 mg/I P: Total as P 665 ma,I Se -Selenium Uq/1
Chromium: Hex 1032 uq/1 Zn -Zinc 46567 UQ/1
Color: True 80 Pt-Co
Cyanide 720 mg/I
Lab Comments:-------------------------------------------------------
GW-54 REV. f/ For Dissolved Analysis -submit filtered sample and write "DIS" in bloc',
EHNR/DEM LABORATORY LAB NO. GG1070
•' . :..,.. VOLATILE ANALYTICAL REPORT
REPORTED BY SCR /5«1:__ SUPEnVISOll
CHECKED BY ~-
DATE
REVIEWED BY -t!.L ENTERED BY
SAMPLE TYPE: WAHR ANALYSIS RESULTS
75-35-4 1, 1-Dichloroethene 0.75 u 96-18-4 1,2,3-Trichloropropane 0.25 u
75-09-2 Methylene Chloride 10 u 108-86-1 Bro mo benzene u
156-60-5 trans-1, 2-Dich!oroethene 0.75 u 95-49-8 2-Chlorotoluene 0.25 u
75-34-3 1, 1-0ichloroethane 0.25 u 106-43-4 4-Chlorotoluene 0.25 u
590-20-7 2, 2-Dichloropropane 0.25 u 541-73-1 1,3-Dichlorobenzene 0.25 u
156-59-4 cis-1,2-Dichloroethene 0.25 u 106-46-7 1 ,4-0ichlorobenzene 0.25 u
67-66-3 Chloroform 0.25 u 95-50-1 1,2-Dichlorobenzene 0.25 u
74-97-5 Bromochloromethane 0.75 u 96-12-8 1,2-Dibromo-3-Chloropropane u
71-55-6 1, 1, 1-Trich!oroethane 0.25 u 120-82-1 1,2,4-Trichlorobenzene 0.25 u
563-58-6 1. 1-Dichloropropene 0.25 u 87-68-3 Hexachlorobutadienc 0.25 u
56-23-5 Carbon Tetrachloride 0.75 u 87-61-6 1,2.3-Trichlorobenzenc 0.75 u
107-06-2 1,2-Dichloroethane 0.25 u 1634-04-4 Methyl-tert-butyl ether 5 u
79-01-6 Trichloroethene 0.25 u 71-43-2 Benzene u
78-87-5 1,2-Dichloropropane 0.25 u 108-88-3 Toluene u
75-27-4 Bro mod ichlor om ethane 0.25 u 100-41·4 Ethyl benzene 1 u
74-95-3 Dibromomethane u 108-38·3 m,p-Xylenes 2 u
10061-01-5 cis-1,3-Dichloropropene 0.25 u 95-47-6 o-Xylene u
10061-02-6 trans-1,3-Dichloropropene 0.25 u 100-42-5 Styrene u
79-00-5 1, 1,2-Trichloroethane 0.25 u 98-82-8 lsopropylbenzene u
127-18-4 Tetrachloroethene 0.25 0.35 103-65-1 n-Propylbenzene u
142-28-9 1.3-Dichloropropane 0.25 u 108-67-8 1,3, 5-Trirnethylbenzene u
124-48-1 Di br ornochlo r om ethane 0.75 u 98-06-6 tert-Butylbenzene u
106-93-4 1,2-Dibromoethane u 95-63-6 1,2,4-Trimethylbenzene u
108-90-7 Chlorobenzene 0.25 u 135-98-8 sec-Butylbenzene u
630-20-6 1, 1, 1 ,2-Tetrach!oroethane 0.25 u 99-87-6 p-isopropyltoluene u
75-25-2 Bromoform 0.5 u 104-51-8 n-Butylbenzene u
79-34-5 1, 1,2,2-Tetrachloroethane 0.75 u 91-20-3 Naphthalene u
. ·. :··:-.-:.:,-.,,: ·.· ,> rng/l rng/l
TOL-Target Ouantitation Limit-Subject to Gasoline Range Estimated Total Petroleum Hydrocarbon 0.25 fJ
change due to instrument sensitivity
T· Tentatively Identified, not confirmed Other purgeables detected_ Detected ,. Estimated Value (up to 10 highest peaks) ug/L
U· Samples analyzed for this compound but not detected
fJ-Sample not analyzed for this compound NO VOLATILE ORGANIC COMPOUNDS
D· Detected below quantitation !imit DETECTED BY GC/PID.
M· GC/MS Analysis performed
COMMENTS:
COUNTY·
QUAD NO:
I./
!REDELL
RErORTTO
COLLECTOR(S) : 0
,_1
0
R
0
0~ ________ Regional Office
DAHLEN
DATE:
rlME:
PURPOSE:
5/15196
LABORATORY ANALYSIS
BOD J\O
COD J ligh 340
COD Low 335
Coliform· Mffo;al31616
Coliform: MF Total 31504
TOC
Turbitity
Residue .. Suspended 530
Total Suspended solids
pH
Alkalinity to pH 4.5
Alkalinity to pH 8 3
Carbona!e
Bicarbonalc
Carbon dioxide
Chloride
Chromium: llell 1032
Color: True 80
Cyanide720
COMMENTS:
ms'L
mg/L
mg/L
/IOOml
1100ml
mg,!
NTU
mg,!,
mg/L
units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
•g/L
'"·
mg/L
Owner:
Location or Site:
Descripliofl of sampling point
Sampling Method:
Remarks·
Diu. Solids 70300
Fluoride 951
Hardness: total 900
I lardness: (non-carb) 902
Phenol, 32730
Specific Cond. 95
Sulfate
Sulfide 745
M8AS
Oil and Grea5e
Silica
Boron
NHJ as N 610
TKN as N 625
X NO2 +N03 as n 630
P: Total as P 665
P04
.S, 9rno 1?
SAMPLE PRIORITY
EjROUTINE □EMERGENCY
ID CHAIN OF CUSTODY
~ SAMPLE TYPE
DAVIDSON REi'{TAI, HOUSE
mg/L
mg/L
mg/L
mg/L
,g/L
uMhos/cm2
mg/L
mg/L
mg/L
mg/L
mg/L
mg/I,
mg/L
1.4 mg/L
mg/L
mg/L
□
Ag-Silver 46566
Al-Aluminum 46557
As-Arsenic 4655 I
!la-Barium 46558
Ca-Calcium 46552
Cd-Cadium 46559
Cr-Chromium 46560
Cu-Copper I 042
Fe-Iron 1045
X I lg-Mercury 7 I 900
K-rotassium 46555
Mg-Magnesium 927
Mn-Manganese 1055
Na• Sodium 929
Ni-Nickel
Pb-Lead 46564
Sc•Sclenium
Zn Zinc 46567
Lab Number 6Gl071
Date Received ; 5/16/96
Time Received 9:00 AM
Received By D.S
•g/L Organochlorinc Pesticides
,g/L Organophosphorus Pesticides
,g/L Nitrogen Pesticides
,g/L
mg/L Acid Herbicides
,g/L
,g!L Scmivo]alilcs
,g/L TPI I-Diesel Range
,g/L
<0.2 ug/L X Volatile Organics (VOA bottle)
mg/L
mg/L TPH-Gasoline Range
•g/L TPH-BTEX Gasoline R:111gc
mg/L
,g/L
,g!L
,g!L
,g/L
6G1071.MAY
GROUNDWATER FIELD/LAB FORM
County ~d.:. !l
Qua·d No L 6 7,,,,..,
Lat. 35--0 '·0-t -;-9")J
Serial No.-~~----0,,,, r--, lc,,,i lJ Long. Q<,-> -" / .LL
Report To: ARO, FRO,~RRO, WaRO, WiRO,
filROUTINE □EMERGENCY
@CHAIN OF CUSTODY
WSRO, Kinston FO~d. Trust, Central Off., Other: ________ _
North Carolina
Department of Environment, Health, and Natural Resources
DIVI_SION OF ENVIRONMENTAL MANAGEMENT-GROUNDWATER SECTION
':::icl-'-'""-1'---'--Cf_,___Time
Rec'd by .. ,.___,__-_,__ From: Bu~. Hand Del.,
Other: ________________ _
Data Entry By: ______ Ck: ______ _
Date Reported: _____________ _
Shipped by: Bus~Couri, Hand Del., Other· P
1"' { /_ 'I I 01 /7ttf! . urpose:
Collector(s): p""-.a.,,.,_ Date turfl, Time /) · d?J Baseline, Complaint, Compliance/ LUST, Pesticide Study, Federal Trust, Other:
FIELD AN~LYSES . .s//f/-S owner }).,U:J.n,,,___ ]~,,J ft 04-Y-, '("'.o';~s:,:-,, Kw~¼ <,, -)
(:rJ.,.;> .J;,..<.."' :] 't;,. 2
e,_1/<-..{1,~ ¼·,.
pH400 ~5-o Spec. Cond.94 3 L. a!Wc Location or site !Zs l.g_:;;.~ Jl>,c,v"-. _ J .
Temp.10 / 5 °c, Odor -Description of sampling point "'if'1J<'"" .-:., S 0 ;,e" /:'I o fy~u... v~ k:
Appearance c{"-"-:z{j· cju-0; Sampling Method ,---'::'l Sample Interval _______ _
I ~-~
Field Analysis By: _ c C, '-'-Remarks--------------------------------------{pumping limo, air !omp. etc.)
LABORATORY ANALYSES
BOD, 310 mqll Diss. Solids 70300 ma/I Aa -Silver 46566 uq/I Organochlorine Pesticides
COO High 340 mg/I Flouride 951 mall Al -Aluminum 46557 uq/I Organophosphorus Pesticides
COD Low 335 mg/I Hardness: Total 900 mnll As -Arsenic 46551 uall Nitroqen Pesticides
Coliform: MF Fecal 31616 /100ml Hardness (non-carb' 902 mn/1 Ba -Barium 46558 uall
Colilarm: MF Total 31504 /100ml Phenols 32730 uall Ca -Calcium 46552 mg/I Acid Herbicides
TOC 680 mgll Soecific Cond. 95 uMhos/cm2 Cd -Cadmium 46559 ua/I
Turbidity 76 NTU Sulfate 945 mnll Cr -Chromium 46560 uall Semivolatile Organics
Residue .. Suspended 530 mg/I Sulfide 745 mq/I Cu -Coooer 46562 uall
Fe -Iron 46563 uall
'x. Ho -Mercury 71900 uqll 7~ Volatile Organics (VOA bollle)
pH 403 unit~ K -Potassium 46555 mg/I
Alkalinity to pH 4.5 410 mg/I Mq -Maqnesium 46554 mq,I TPH -Gasoline Range
Alkalinity to pH 8.3 415 mgll Mn -Manqanese 46565 uq/I TPH -BTEX Gasoline Range
Carbonate 445 mg/I NH as N 610 mall Na • Sodium 46556 mq/I
Bicarbonate 440 mall TK/\1 .. ,.. N lYH: -"" Ni -Nickel uall /
Carbon dioxide 405 mgll IX NO +NO as N 630 mnll · Pb -Lead 46564 urul I/
Chloride 940 mg/I P: Total as P 665 mnll Se -Selenium uq/I
Chromium: Hex 1032 UQII Zn -Zinc 46567 uq/I
Color: True 80 Pt-Co
Cyanide 720 mgll
Lab Comments:----------------------------------------------------------
GW-54 REV. f(:.
'-.,
For Dissolved Analysis• submit liltered sample and write "DIS" in bloc',
'-----
F.tPORTED 6Y
CHECKED DY
SAMPLE TYPE:
75-35,4
75·09-2
156-60-5
75-34-3
590-20-7
1 56-59-4
67-66-3
74-97-5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79-34-5
TOL-
T-
E-
WATER
1, 1-Dichloroethene
Methylene Chloride
trans-1 ,2-Dichloroethene
1, 1 -Dichloroethane
2, 2-0ichloropropane
cis-1,2-Dichloroethene
Chloroform
Bromochloromethane
1, 1, 1-Trich!oroethane
1, 1-Dichloropropcne
Carbon Tetrachloride
1,2-Dichloroethane
Trichloroethene
1,2-0ichloropropane
Bromodi chi or a methane
Dibromomethane
cis-1,3-Dichloropropene
trans-1,3-0ichloropropene
1, 1,2-Trichloroethane
Tetrachloroethene
1,3-Dichloropropane
Dibromochloromethane
1 ,2-Dibromoethane
Chlorobenzene
1, 1.1,2-Tetrachloroethane
Bromoform
1, 1,2,2-Tetrachloroethane
Target Ouantitation Limit-Subject to
change due to instrument sensitivity
Tentatively Identified, not confirmed
Estimated Value
0.75
10
0.75
0.25
0.25
0.25
0.25
0.75
0.25
0.25
0.75
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.75
1
0.25
0.25
D.5
0.75
U-Samples analyzed for this compound but not detected
N-
D-
M-
Sample not analyzed for this compound
Detected below quantitation limit
GC/MS Analysis performed
EHNR/DEM LABORATORY
VOLATILE ANALYTICAL REPORT
DT
ANAL YS1S RESULTS
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
96-18-4
108-86-1
95-49-8
106-43-4
541-73-1
106-46-7
95-50-1
96-12-8
120-82-1
87-68-3
87-61-6
1634-04-4
71-43-2
108-88-3
100-41-4
108-38-3
95-47-6
100-42-5
98-82-8
103-65-1
108-67-8
98-06-6
95-63-6
135-98-8
99-87-6
104-51-8
91-20-3
1,2,3-Trichloropropane
Bromobenzene
2-Chlorotoluene
4-Chlorotoluene
1,3-0ichlorobenzene
. 1,4-0ichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
Hexachlorobutadiene
1,2,3-Trichlorobenzene
Methyl-tert-buty! ether
Benzene
Toluene
Ethyl benzene
m,p•Xylenes
a-Xylene
St'{rene
lsopropylbenzene
n-Propylbenzene
1,3,5-Trimethylbenzene
tert-Butylbenzene
1,2,4-Trimethy!benzene
sec-Butylbenzene
p-isopropyltoluene
n-_Butyibenzene
Naphthalene
Other purgeables detected
(up to 10 highest peaks)
NO VOLATILE ORGANIC COMPOUNDS DETECTED BY
GC/PJD.
LAB NO. 6G1071
SUPERVISOR
DATE
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.75
5
2
1·
1
mg/L
0.25
mg/L
Detected
ug/L
u .
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
N
COMMENTS:------------------------------------------------'-----------------
(
JUNTY
JADNO:
\: 31
CJ>ORTTO
JLLECfOR(S)
\TE:
_,_rn_o _________ Regional Office
DAIILER
4117196
YIE·
IRPOSE:
;\IJORATORY ANALYSIS
DOD 3!0
COD High 340
COD Low335
Coliform: MF Fecal 31616
Colifonn: MF Total 31504
TOC
Turbitity
Residue., Su5pended 530
Total Su~pended solids
pH
Alkalinity to pH 4.5
Alkalinity to pH 8.3
Carbonate
Bicarbonate
Carbon dioxide
Chloride
Chromium: Hex 1032
Color: True 80
Cyanide720
lMMENTS:
m,;IL
m,;IL
m,;IL
1100ml
1100ml
mg/l
ITTU
m,;IL
m,;IL
u11i1s
m,;IL
m,;IL
mg/L
m,;IL
m,;IL
m,;IL
"&'L
c.u.
m,;IL
Owner:
Location or Site:
Description of sampling point
Sampling Method:
Remarks:
Diss. Solids 70300
Fluoride 95 I
11:udness: total 900
I !ardness: (non•carb) 902
Phenols 32730
Specific Cond. 95
Sulfate
Sulfide 745
Ml3AS
Oil and Grease
Silica
Boron
NH3asN610
TKN asN 625
N02 +N03 as n 630
P: Total as P 665
P04
DIVISION OF ENVlRONl\lENTAL i\1ANAGE1\IENT
Chrmi:itry L11borPlory Rrpod f Ground W111rr Quality
SAMrLE rRIQRJTY
[8:JROlITJNE
~ CIIAJNOFCUSTODY
~ SAMPLE TYPE
JOHN LAMBERT
mg/l,
m,;IL
m,;IL
m,;IL
,,;IL
uMhos/cm2
m,;IL
m,;IL
m,;IL
m,;IL
m,;IL
m,;IL
m,;IL
mg/I,
m,;IL
mg/l,
□EMERGENCY
□
Ag-Silver 46566
X Al-Aluminum 46557
As-Arsenic 4655 I
Ba-Barium 46558
Ca-Calcium 46552
Cd·Cadium 46559
Cr-Chromium 46560
Cu-Copper 1042
Fe-Iron 1045
X I lg-Mercury 71900
K-Potassium 46555
Mg-t-fagnesium 927
Mn-Manganese 1055
Na• Sodium 929
Ni-Nickel
Pb-Lead 46564
Sc-Selenium
Zn_Zinc 46567
,,;IL
200 ,,;IL
,,;IL
,,;IL
m,;IL
,,;IL
,,;IL
,,;IL
,,;IL
<0.2 ,,;IL
m,;IL
m,;IL
,,;IL
m,;IL
,,;IL
,,;IL
,g/L
,,;IL
Lab Numbcer
Dale Recci,·cd
Time RecciveJ
Received By
Released By :
Date reponed :
Organochlorinc Pesticides
Organophosphorus Pesticides
Nitrogen Pesticides
Acid Herbicides
Semivolatilcs
TPII-Dicsel Range
6G776
4118196
8:45 AM
OS
Volatile Organics (VOA bonlc)
TPl 1-Gasolinc Range
TPl 1-BTEX Gasoline Range
6G716APR
North Carolina
GROUNDWATER FIELD/LAB FORM Department of Environment, Health, and Natural Resources
DIVISION OF ENVIRONMENTAL MANAGEMENT-GROUNDWATER SECTION
County yuk,l(
Quad No (. Cc. 7 <' J Serial No. _____ _
,...,, y·31 . '•'N' C,-~ .·-:,• ) •• ' Lat. ? J o(;:; Long. •--i:J ~s~J C .... '--'-""
Report To: ARO, FRO.~ RRO, WaRO, WiRO,
,f) t'i II ~._:"F~ f;-"'\ ~
SAMPLE PRIORITY
~OUTINE □EMERGENCY
J8'CHAIN OF CUSTODY
WSRO, Kinston FO, Fed. Trust, Central Ott., Other: ________ _
Shipped by: Bus , Hand Del., Other_·--------~---
Lab Number --'rt~e':'-..c:k--'-.-'"""--....-----:--,-,---
0 "'==,._,~~-111: , oun r, an Del.,
Other: ________________ _
Data Entry By: ______ Ck: ______ _
Date Reported: _____________ _
Collector(s): -cJ,"""'..u._,_._ __ Date '/µ1(5:( Purpose:~~ -Ll!...l.:..;__,;:'-'~'-·-___ Baseline, ~t: Compliance, LUST, Peslicide Sludy, Federal Trust, Other: _______ _
, ,wcl11 or.e) ;-( L Time
FIELD ANALYSES Owner ;Td,1, Le;.., i,.vf well kjn-& n ·vv '
pH4~::iv-r:.s-Spec. Cond.94 ___ at25°C
Temp.10 _ ____=cc..---°C Odor _____ _
Appearance C (, c: -I << (;.d., cc
Location or site -----------------~-----------------
Description of sampling point -""l:.,_,_d..1.cs...,,i..1., _ _,_,rL, ~eo· c1C...,,'--~---";.;=-c!Y-"""c:-:..,<---ff:u.l'.,,l-:::::.· -----------
Sampling Method _______ ,,.....,::..,.'~'---------Sample Interval _______ _
Field Analysis By: _£)µ,,~:....· ..._(___,(,._,~~------
LABORATORY ANALYSES
Remarks 1(1,.,,o..... a...<✓-:c....c,e..,J {kiiiiiP.-da,1ur. 111c l
-' / ~"mpmg ,mo, ,ot,mp "')
BOD 310 ma/I Diss. Solids 70300 m-'I Ao -Silver 46566 un/I OrQanochlorine Pesticides
COD High 340 mg/I Flouride 951 m.vv ./ Al -Aluminum 46557 unll Organophosphorus Pesticides
COD Low 335 ma/I Hardness: T olal 900 m~'I As -Arsenic 46551 un/I Nitroaen Pesticides
Coliform: MF Fecal 31616 /100ml Hardness (non-carb) 902 mn/I Ba• Barium 46558 unll
Coliform: MF Total 31504 1100ml Ehenols 32730 ug/I Ca• Calcium 46552 ' mn,I Acid Herbicides
TOG 680 mail Snecific Cond. 95 uMhos/cm2 Cd -Cadmium 46559 un/I
T urbidily 76 NTU Sulfate 945 mnll Cr -Chromium 46560 un/I Semivolatile Organics
Residue., Suspended 530 mg/I Sulfide 745 mn1I Cu • Coooer 46562 ua/I -Fe -Iron 46563 ua/I
' v Hg -Mercurv 71900 ua,I Volatile Organics (VOA bollle)
pH 403 unit~ K -Potassium 46555 mn/I
Alkalinity to pH 4.5 410 mg/I Mq -Maqnesium 46554 mail TPH -Gasoline Range
Alkalinity to pH 8.3 415 mg/I Mn -Man□anese 46565 ua/I TPH -BTEX Gasoline Range
Carbonate 445 mg/I NH as N 610 mn/I Na -Sodium 46556 ma/I
Bicarbonate 440 mn/I TKN se N Coe --" Ni -Nickel un,I
Carbon dioxide 405 ma/I NO + NO as N 630 ma/I Pb -Lead 46564 un,I
Chloride 940 mg/I P: Total as P 665 mnl, Se -Selenium Uail
Chromium: Hex 1032 Ua/I Zn -Zinc 46567 u01I
Color: True 80 Pl-Co
Cyanide 720 mg/I
Lab Comments:----------------------------------------------------------
GW-54 r'. l/93 For Dissolved Analysis -submit tillered sample and write "DIS" i~ . ___ ,,
JNTY
·\DNO:
IREOELL
'ORT TO 0P0110Wcc_= ________ Resional omee
.LECTOR(S) : ~D~A~ll~L=E=.Rc· ______ _
rE: ◄117/96
E
lPOSE:
,BORATORY ANALYSIS
BOD J IO
COD High 340
COD Low 335
Coliform: MF fecal 31616
Colifonn: MFTotal3!504
TOC
Turbitity
Residue., Suspended 530
Total Suspended solids
pH
All<nlinity lo pll 4.5
Alkalinity to pH 8.J
Carbonate
Bicarbonate
Carbon dio:<ide
Chloride
Chromium: Hex 1032
Color: True 80
Cyanide 720
,IMENTS:
mg/L
mg/L
mg/L
1100ml
/!00ml
mwl
NTU
mg/L
mg/L
units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
,g/L
'·"
mg/L
Owner:
l,ocation or Site:
Description of =piing point
Sampling Method·
Remarks:
Diss. Solids 70300
Fluoride 951
Hardness: total 900
Hardness: (non-carb) 902
Phenols 32730
Specific Cond. 95
Sulfate
Sulfide 745
MBAS
Oil and Grease
Silica
Boron
N/13 as N 610
TKN as N 625
NO2 +NO) as n 630
r: Total as P 665
P04
\: 37
DIVISION OF ENVIRONI\IENTAL i\.lANAGEi\.lENT
Chemblry Laboratory Report I GrounJ \\'alu Quality
Sf._HCT._E PRIQR[TY
~ROUTINE
~ Cl!AINOFCUSTODY
EJ SAMPLE TYPE
JOIIN LAMBERT
mg/L
mg/L
mg/L
mg/L
,g/L
uMhos/cm2
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
□
Ag-Silver 46566
X Al-Aluminum 46557
As-Arsenic 4655 I
Ba-Barium 4655B
Ca-Calcium 46552
Cd-Cndium 46559
Cr-Chromium 46560
Cu-Copper 1042
Fe-Iron 1045
X tlg-Me,.;ury 71900
K-Potnssium 46555
Mg• Magnesium 927
Mn-Manganese 1055
Na· Sodium 929
Ni-Nickel
Pb-Lend 46564
Se-Selenium
Zn Zinc 46567
,g/L
180 ,g/L
,g/L
,g/L
mg/L
,g/L
,g/1.
,g/L
,g/L
<0.2 ,g/L
mg/L
mg/L
,g/L
mg/L
,g/1.
,g/L
,g/L
,g/L
Lab Number
Dale Recei,·cJ
Time Recei,·eJ
Received Dy
Organochlorine Pesticides
Organophosphorus Pesticides
Nitrogen Pesticides
Acid Herbicides
Semi,·o!atiles
TPII-Diesel Range
6G777
4118196
8:45AM
OS
Volatile Organics {VOA bottle)
TPII-Gasoline Range
TP/1-UTEX Gnsoline Range
6Gl17APR
Norlh Carolina
GROUNDWATER FIELD/LAB FORM Dcpartmcnl of Environment, Health, and Naturnl Resources
DIVISION OF ENVIRONMENTAL MANAGEMENT. GnOUNDWATEn SECTION
County ...:C,. ~ti
Quad No '-(, ]y J Serial No. _____ _
Lat. °? \-o,f J I o .. ; 1~N Long. ,o4,., ·> ·:~ C .L4 l...>
Report To: ARO, FRO,~ RRO, WaRO, WiRO,
SAMPLE PRIORITY
Qi]'ROUTINE □EMERGENCY
[2QcHAIN OF CUSTODY
WSRO, Kinston FO, Fed. Trust, Central Off., Other: ________ _ 0
Shipped by: Bus~ Hand Del., Other· ___________ _
Cottector(s): b.,-l..4, Date t(rzl ?,(, Time //c'-i',----
Purpose: .,,,,,--:)
Baselir_,e, Cc[wphflnt, Compliance
EIELP ANALYSES 7 owner -C. L
Date Receil""'(A5/-~f-'-"'~
Rec'd by:_.,....,~~-
Other: ________________ _
Data Entry By: ______ Ck: ______ _
Date Reported: _____________ _
pH,00 ~fo-~-:.:(" Spec. Cond.94 ___ at25°C Location or site -------~---~~-----.------------------
Description of sampling point -~h~'~-1:~0 ~-·-½ ~~j~'~~~L~~<'--'1r-<~·<-c~7f-· +i-<~· ~<-,: ____________ _ Temp.10 -0 c , Odor ______ _
Appearance <--G..,:;.__i_""-~~ C. ./?'
Field Analysis By: -J>b).:;:.,.a:..-4-(.,,J~---------
LABORATORY ANALYSES
Sampling Method --------.@-===-------Sample Interval _______ _
LJ [ ~b.1Jiqr,e\c) Remarks ,,,, .. ,.3, 2.-s-lv<..:<'
I (pumping time, illr lemp. eLc.)
BOD. 310 ma/I Diss. Solids 70300 mn/l Aq • Silver 46566 ua/I Organochlorine Pesticides
COD High 340 mg/I Flouride 951 mQ/I i/ Al • Aluminum 46557 ug/I Organophosphorus Pesticides
COD Low 335 mnn Hardness· Total 900 mn/l As • Arsenic 46551 ua/I Nitrogen Pesticides
Coliform: MF Fecal 31616 /100ml Hardness tnon-r::arbl 902 mail Ba -Barium 46558 Ua/I
Coliform: MF Total 31504 /100ml Phenols 32730 uail Ca -Calcium 46552 mq/I Acid Herbicides
TOG 680 mail Snecific Cond. 95 uMhos/cm2 Cd -Cadmium 46559 unn
Turbidily 76 NTU Sulfate 945 mail Cr -Chromium 46560 . ua/I Semivolatile Organics
Residue., Suspended 530 mg/I Sulfide 745 mail Cu -Coeeer 46562 ugil
Fe -Iron 46563 uqil
{,/ Hq • Mercury 71900 ug/I Volatile Organics (VOA bollle)
pH 403 unit~ K -Potassium 46555 mg,I
Alkalinity lo pH 4.5 410 mg/I Mo -Maqnesium 46554 mQ/I TPH -Gasoline Range
Alkalinity to pH 8.3 415 mg/I Mn -Manqanese 46565 uq,I TPH · BTEX Gasoline Range
Carbonate 445 mg/I NH as N 610 mall Na • Sodium 46556 mg,I
Bicarbonate 440 mQ/I ; TK" 0 s N <O< ~n,I Ni· Nickel LIO/I ""1
Carbon dioxide 405 mOI I NO +NO as N 630 mail Pb · Lead 46564 uail
Chloride 940 mg/I P: Total as P 665 mail Se -Selenium ug,I
Chromium: Hex 1032 ug1I Zn • Zinc 46567 UQ/I
Color: True 80 Pt-Co
Cyanide 720 mg/I
Lab Comments:----------------------------------------------------------
GW-54 F i/93 For Dissolved Analysis -submit filtered sample and write MDIS" i~,.-' · -:k.
JUNTY
UADNO:
IREDELL
RECE!VED/EHHR
OHi. GROUMD WATER SEC.
DIVISION OF ENVIRONi\lENTAL J\lANAGEl\lENT
96 JUL 11 ~!'1\\:32 Chemi,try Laboratory Report/ Gro11nd \\'ater Quality
SAMPLE PRIQRIJY
E_]ROUTINE □EMERGENCY
~~~:-:;iR(S) : c~c'~c',c~cLcEcN,--------Rcgional Office ~ CHAIN OF CUSTODY □ A.TE· 4115/96
ME:
JRPOSE:
.ABORATORY ANALYSIS
BOD 310 mg/L
COD l-lig.h 340 ms'L
COD Low3J5 mg/L
Coliform: MF Fecal 31616 1100ml
Colifonn: MF Total 31504 1100ml
TOC mg/I
Turbitity NTU
Residue., Suspended 530 mg/L
Total Suspended solids mg/L
pH units
Alkalinity to pH 4.5 mg/L
Alkalinity to pH B.J mg/L
Carbonate mg/L
Dicarbon:ite mg/L
Carbon dioxide mg/L
Chloride mg/L
Chromium: I-lex 1032 og/1.
Color: True 80 c.u.
Cyanide 720 mg/L
OMMENTS: •• NO SAMPLE PER JCF
Owner:
Location or Site:
Description of sampling point
Sampling Method:
Remarks·
Diss. Solids 70300
Fluoride 951
Hardness: total 900
l-lardness: (non-erub) 902
Phenols 32730
Specific Cond. 95
Sulfate
Sulfide 745
MBAS
Oil and Grease
Silica
Boron
NIIJ:isN610
TKN as N 625
NO2 +NOJ as n 6)0
P: T ot111 as P 665
P04
~ SAM~LE TYPE
LAMBERTI! CONSTRUCTION
ms'L Ag-Silver 46566
mg/L Al-Aluminum 46557
mg/L As-Arsenic 46551
mg/L 811-lhrium 46558
og/L Ca-CaJeium 46552
uMhos/cm2 X Cd-C.ulium 46559
mg/L Cr-Chromium 46560
mg/L Cu-Copper 1042
mg/L Fe-Iron 1045
mg/L X Hg-Mercury 71900
mg/L K-Potassium 46555
Mg-Magnesium 927
Mn-Manganese 10S5
mg/L Na-Sodium 929
ms'L Ni-Nickel
mg/L X Pb-Lead 46564
mg/L Sc-Selenium
mg/L Zn Zinc 46567
Lab Number 6G708
Dale Received : 4/16/96
Time Received : 9:35 AM
Received By JG
Released By · G-5
Date reported 7 / i I VJ{.,;
og/L Organochl(lrine Pesticides
og/L Organophosphorus Pesticides
og/L Nitmgcn Pesticides
og/L
mg/L Acid Herbicides .. og/L
og/L X Scmi,·olati!cs
og/L TPH-Dicscl Range
og/L .. os'L Volatile O1gruiics (VOA bo1tle)
mg/L
mg/L X TP!l-Gasoline Range
og/L TPII-BTEX Gasoline Range
mg/L
og/L .. os'L
og/L
os'L
North Carolina
GROUNDWATER FIELD/LAB FORM Department of Environment, Health, and Natural Resources
DIVISION OF ENVIRONMENTAL MANAGEMENT-GROUNDWATER SECTION
County -::z:;,e__,,f__g (/
Quad No (_ b ~ Serial No. ______ _
Lat. »•'I;; '1:.··';J Long. eo~,CB'/., 11 l.J
r t,~STODY
SAMPLE PRIORITY 0
8:SROUTINE □EMERGENCY
~HAIN OF CUSTODY
Shipped by: Bus, Gour' , and Del., Other_· __________ _
Lab Number {o<2}_ 70 ~
Date R~(/~/"?0:fime:...=~q__,_._.,,· ~'---
Rec'd~'-+---From: Bu Courier Ha Del.,
Other: _______________ _
Data Entry By: ______ Ck: ______ _
Date Reported: _____________ _ Report To: ARO, FRO,~RO, WaRO, WiRO,
WSRO, Kinston ~FO, Fed Trust, Central Off., Other:
Collector(s): 1.)c;,'1.,,,, Date 'f J:'>L¼ Time -Baselin , Complain, Compliance, LUST, Pesticide Study, Federal Trust, Other: _______ _ >-. { / -(a fl/ . J <'.J Purpose9· -
· 7 I ·r --~
FIELD ANALYSES . Owner L-.,.,, k~+L --&"-,:::\ ,-'1...,< +w ,
pH400 ~spec. Cond.94 --at 25° C Location or site ,3,_,__ (c ✓ . s f
Temp.10 ___ -_-_-_0 c. Odor_.--______ Description of sampling point ~-------------------------~---
Appearance Sampling Method /, «~ d c. u O"✓ Sample Interval J'-3-.> -'
< . _.J. /. c.?tPump, Oil.11'11. eLC) /
FieldAnalysisBy: Remarks --'""'-;-«'l,._ L<-:, ~ 3/ LY"'--" 141 ,,,_,, vo~/21112~ :'G~:I cl., ,P!t-~-AS
LABORATORY ANALYSES (p"mp,o,m,.,,i,mp "') I -f-.5 l--'o,A J
BOD, 310 mQ/I Diss. Solids 70300 mnil An • Silver 46566 unit Orqanochlorine Pesticides
COD High 340 mg/I Flouride 951 m~,I Al • Aluminum 46557 ua/I Organophosphorus Pesticides .
COD Low 335 m()il Hardness: Total 900 ma/I As • Arsenic 46551 ua/I Nitrogen Pesticides
Coliform: MF Fecal 31616 /100ml Hardness {non-carb) 902 ma/I Ba • Barium 46558 un/1
Calilorni: MF Total 31504 /100ml Phenols 32730 U□il Ca -Calcium 46552 ma/I Acid Herbicides
TOG 680 m()il Saecific Cond. 95 uMhos/cm2 >< Cd -Cadmium 46559 V ua/I
Turbidity 76 NTU Sulfate 945 mQ/I Cr• Chromium 46560 ua/I i>< Semivolatile Organics
Residue., Suspended 530 mg/I Sulfide 745 mQ/I Cu -Cooner 46562 UQ/I
Fe -Iron 46563 Uq/l
--x Hq • Mercury 71900 ,k uq/l Volatile Organics (VOA bottle)
pH 403 units K -Potassium 46555 . mg/I
Alkalinity to pH 4.5 410 mg/I Ma -Maanesium 46554 ma/I >< TPH • Gasoline Range
Alkalinity to pH 8.3 415 mg/I Mn • Manaanese 46565 UQ/I TPH -BTEX Gasoline Range
Carbonate 445 mg/I NH as N 610 mQ/I Na -Sodium 46556 mQ/I
Bicarbonate 440 ma/I TKfl.1 --N ~?c:;; --" Ni -Nickol unil I
Carbo'ri'dioxide 405 mQ/I NO +NO as N 630 matt >< Pb -Lead 46564 ± UQ/I \ I
Chloride 940 mg/I P: Total as P 665 mrul Se -Selenium un/1 \}
Chromium: Hex 1032 UQ/I Zn -Zinc 46567 un/1
Colar: True so Pt-Co
Cyanide 720 mg/I
GW-54 REV. 6'93 For Dissolved Analysis• submit filtered sample and write "DIS" in bloc~ .. ·
c~
EHNR/DEM LABORATORY LAB NO. 6G708
,1 ✓ VOLATILE ANALYTICAL REPORT
REPORTED BY SUPERVISOR
CHECKED BY i) DATE
REVIEWED BY tf/(!,,
ENTERED BY
SAMPLE TYPE; SOIL ANALYSIS RESULTS
75.35.4 1, 1-Dichloroethene 22 N 96-18-4 1,2,3-Trichloropropane 7.5 N
75-09-2 Methylen~ Chloride 300 N 108-86-1 Bromobenzene 30 N
156-60-5 trans-1,2-Dichloroethene 22 N 95-49-8 2-Chlorotoluene 7.5 N
75-34-3 1. 1 -Dichloroethane 7.5 N 106-43-4 4-Chlorotoluene 7.5 N
590-20-7 2, 2-Dichloropropane 7.5 N 541-73-1 1, 3-0ichlorobenzene 7.5 N
156-59-4 cis-1,2-Dichloroethene 7.5 N 106-46-7 1,4-Dichlorobenzene 7.5 N
67-66-3 Chloroform 7.5 N 95-50-1 1,2-Dichlorobenzene 7.5 N
74-97-5 Bromochloromethane 22 N 96-12-8 1,2-Dibromo-3-Chloropropane 30 N
71-55-6 1, 1, 1-Trichloroethane 7.5 N 120-82-1 1,2,4-Trichlorobenzene 7.5 N
563-58-6 1, 1-0ichloropropene 7.5 N 87-68-3 Hexachlorobutadiene 7.5 N
56-13-5 Carbon Tetrachloride 22 N 87-61-6 1,2,3-Trichlorobenzene 22 N
107-06-2 1,2-Dichloroethane 7.5 N 1634-04-4 Methyl-tert-butyl ether 150 N
79-01-6 Trichloroethene 7.5 N 71-43-2 Benzene 30 N
78-87-5 1,2-Dichloropropane 7.5 N 108-88-3 Toluene 30 N
75-27-4 Br omodlchl or om ethane 7.5 N 100-41-4 Ethyl benzene 30 N
74-95-3 Dibromomethane 30 N 108-38-3 m,p-Xylenes 60 N
10061-01-5 cis-1,3-Dichloropropene 7.5 N 95-47-6 a-Xylene 30 N
10061-02-6 trans-1,3-Dichloropropene 7.5 N 100-42-5 Styrene 30 N
79-00-5 1, 1,2-Trichloroethane 7.5 N 98-82-8 lsopropylbenzene 30 N
127-18-4 Tetrachloroethene 7.5 N 103-65-1 n-Propylbenzene 30 N
142-28-9 1 ,3-Dichloropropane 7.5 N 108-67-8 1, 3. 5-T rimethylbenzene 30 N
124-46-1 Di bro mochlo r omet ha ne 22 N 98-06-6 tert-Butylbenzene 30 N
106-93-4 1,2-Dibromoethane 30 N 95-63-6 1,2.4-Trimethylbenzene 30 N
108-90-7 Chlorobenzene 7.5 N 135-98-8 sec-Butyl benzene 30 N
630-20-6 1, 1, 1,2-Tetrachloroethane 7.5 N 99-87-6 p-isopropyltoluene 30 N
75-25-2 Bromoform 15 N 104-51-8 n-Butylbenzene 30 N
79-34-5 1, 1,2,2-Tetrachloroethane 22 N 91-20-3 Naphthalene 30 N
TOL-Target Quantitation limit-Subject to lli:Irr~:::'ii~~.::~:=~·sli't~fi~-t{:=~;;:.:i:t.;};I~:~=,,_~;:~·;:;-~'::~-~:~:::--,
mg/L mg/L
7.5 u
change due to instrument sensitivity
T-Tentatively Identified, not confirmed Other purgeables detected Detected
E-Estimated Value (up to 1 0 highest peaks) ug/L
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound
0-Detected below quantitation limit
M-GC/MS Analysis performed
COMMENTS: ________________________________________________________________
_
__ __,.
.
EHNR/DEM LABORATORY LAB NO. ~G7tJf
~ SEMI-VOLATILE ANALYTICAL REPORT
REPORTED BY SUPERVISOR "R"~
CHECKED BY DATE ·!Jlj~ REVIEWED BY p ENTERED BY . fl
SAMPLE TYPE: SOIL ANALYSIS RES UL TS DATE ey340G>
62-53-3 ANILINE 660 u 606-20-2 2,6-0INITROTOLUENE 660 u
108-95-2 PHENOL 660 u 99-09-2 3-NJTROANlLINE 3300 u
111-44-4 BIS{2-CHLOROETHYL) ETHER 660 u 83-32-9 ACENAPHTHENE 660 u
95-57-8 2-CHLOROPHENOL 660 u 51-28-5 2,4-DINITRO PHENOL 3300 u
541-73-1 1,3-DICHLOROBENZENE 660 u 100-02-7 4-NJTRO PHENOL 3300 u
106-46-7 1,4-DICHLOROBENZENE 660 u 132-64-9 DIBENZOFURAN 660 u
100-51-6 BENZYL ALCOHOL 1300 u 121-14-2 2,4-DINITAOTOLUENE 660 u
95-50-1 1 ,2-DICHLOROBENZENE 660 u 84-66-2 DIETHYL PHTHALATE 660 u
95-48-7 2-METHYL PHENOL 660 u ·1005-72-3 4-CHLOROPHENYL PHENYL ETHER 660 u
108-60-1 8I5(2-CHLOROISOPROPYL) ETHER 660 u 86-73-7 FLUORENE 660 u
106-44-5 4-METHYL PHENOL 660 u 100-01-6 4-NJTROANILINE 3300 u
621-64-7 N-NITAOSO-D1-N-PAOPYLAMINE 660 u 534-52-1 4,6-DINITR0-2-METHYL PHENOL 3300 u
67-72-1 HEXACHLOAOETHANE 660 u 86-30-6 N-NITROSODIPHENYLAMINE 660 u
99.95.3 NITROBENZENE 660 u 101-55-3 4-BROMOPHENYL PHENYL ETHER 660 u
78-59-1 ISOPHOAONE 660 u 118-74-1 HEXACHLOROBENZENE 660 u
88-75-5 2-NITRO PHENOL 660 u 87-86-5 PENTACHLORO PHENOL 3300 u
105-67-9 2,4-DIMETHYL PHENOL 660 u 85-01-8 PHENANTHRENE 660 u
65-85-0 BENZOIC ACID 3300 u 120-12-7 ANTHRACENE 660 u
111-91-1 8I5(2-CHLOROETHOXY) METHANE 660 u 84-74-2 0I-N-BUTYL PHTHALATE 660 u
120-83-2 2,4-0ICHLORO PHENOL 660 u 206-44-0 FLUORANTHENE 660 u
120-82-1 1,2.4-TRICHLOROBENZENE 660 u 129-00-0 PYRENE 660 u
91-20-3 NAPHTHALENE 660 u 85-68-7 BUTYLBENZYL PHTHALATE 660 u
.106-47-8 4-CHLOROANILINE 1300 u 91-94-1 3,3'-DICHLOROBENZIDINE 1300 u
87-68-3 HEXACHLOROBUTAOIENE 660 u 56-55-3 BENZO(A)ANTHRACENE 660 u
59-50-7 4-CHLOA0-3-METHYL PHENOL 1300 u 218-01-9 CHRYSENE 660 u
91-57-6 2-METHYL NAPHTHALENE 660 u 117-81-7 BIS(2-ETHYLHEXYL) PHTHALATE 660 u
77.47.4 H EXACHLOROCYCLOPENT AOIENE 660 u 117-84-0 0I-N-OCTYL PHTHALATE 660 u
88-06-2 2,4,6-TRICHLORO PHENOL 660 u 205-99-2 BENZO(BJFLUORANTHENE 660 u
95.95.4 2,4,5-TRICHLORO PHENOL 660 u 207-08-9 BENZO(KJFLUORANTHENE 660 u
91-58-7 2-CHLORO NAPHTHALENE 660 u 50-32-8 BENZO(AJPYRENE 660 u
88-74-4 2-NITROANILINE 3300 u 193-39-5 INOENO( 1,2,3-CDJPYRENE 660 u
131-11-3 DIMETHYL PHTHALATE 660 u 53-70-3 DlBENZO{A,H)ANTHRACENE 660 u
208-96-8 ACENAPHTHYLENE 660 u 191-24-2 BENZO(G,H,IJPERYLENE 660 V
SEMIVOLATILE ORGANICS REPORT -DEM LAB PAGE 2
UNIDENTIFIED 490 E
UNIDENTIFIED 440 E
LAB NO.
TOL-Target Quantitation Limit-Subject to
change due to instrument sensitivity
T-Tentatively Identified, estimated concentration
E-Estimated Value
U-Samples analyzed fOr this compound but not detected
N-Sample not analyzed for this compound
0-Detected below quantitation limit
H-Holding time exceded
COMMENTS, ___________________________________________________ _
COUNTY
QUAD NO:
IREDELL
REPORT TO c'c'c"aOc__ ________ Regional Office
COLLEC\"Olt(S) : 0n~A~l~IL~l~~N.:_ _____ _
DATE: 4/'l/96
TIME:
PURPOSE:
LABORATORY ANALYSIS
800310
COD l ligh 340
COD Low 335
Coliform: MF fecal 31616
Coliform: MF Total 31504
TOC
Tmbi1i1y
Residue., Suspended 530
Total Suspended solids
pll
Alkalinity to pt\ 4.S
Alk:ilinity to pl I 8 3
Crubonatc
Di carbonate
Carbon dioxide
Chloride
Chromium: Jle:'t IOJ2
Color: True SO
Cyanide 720
C0/',1!\IENTS:
mg/L
mg/L
mg/L
/lOOml
1100ml
mg/1
NTU
mg/L
mg/L
units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
,g/L
'"
mg/L
Owner:
Location or Site:
Dcsc1 iplion of sampling point
Sampling Method:
Remarks·
Diss. Solids 70JOO
Fluoride 95 I
11:irdness: total 900
H:irdness: (non-c:irb) 902
Phenols 32730
Specific Cond. 95
Sulfate
Sulfide 745
MBAS
Oil and Grease
Silica
Boron
Nll3uN610
TKN as N 625
X NO2 +NOJ as n 630
P: To1al as P 665
P04
lll\'ISION OF ENVIHONMENT,\L :\IANAGEi\lENT
Chem is try Lnhorntory Report I Grnuntl \~'nter Qualily
SAMPLE PRIORITY
IKJROUTINE
BJ CIIA[NOFCUSTODY
0 SAMPLE TYPE
IJIJ EIJFOI.A RO,\ll
mg/L
ms.IL
mg/L
mg/L
,g/L
uMhos/cm2
myL
mg/L
mg/1,
mg/L
mgll,
mg/L
mg/L
0.50 mg/L
mg/L
mg/L
□EMERGENCY
□
Ag-Silver 46566
1\1-Aluminum 46557
As-Arsenic 4655 I
lla-ilarium 4655S
Ca-Calcium 46552
Cd-Cadium 46559
Cr-Chromium 46560
Cu-Copper 1042
Fe-Iron 1045
X I lg-Mercury 71900
K-Potassium 46555
Mg-Magnesium 927
Mn-Manganese I 055
Na-Sodium 929
Ni-Nickel
Pb-Le:id 46564
Se-Selenium
Zn Zinc 46567
,yL
ug/L
,g/L
,gll,
mg/L
,gll,
"g/L
,g/L
,g/L
<0.2 ug/L X
mg/L
mg/L
,g/L
mg/L
"g/L
"g/L
,g/L
"g/L
Lab Number
Dale Received
Time Received
Recei\·ed By
Released Dy
Organochlorine Pesticides
Organophosphorus Pesticides
Nitrogen Pesticides
Acid I lerbicides
Semivolati!es
TPII-Diesel Range
6G669
4/10196
10:20 AM
JG
Volatile Organics (VOA bottle)
TPll•Gasoline Range
TPll-nTEX Gasoline Range
.,
6G669APR
.-----------------------------------------------------------North Carolina
GROUNDWATER FIELD/LAB FORM
Counly ___L".c~( l--------------
Ouad No Lb 13 <" Serial No _______ _
Lat. 3SJ'fJ' /t..,''N Long. 80°:{// a5''cJ
Report To: ARO, FRO,~ ARO, WaRO, WiRO,
SAMPLE PRIORITY
~ROUTINE □EMERGENCY
-@CHAIN OF CUSTODY
WSRO, Kinston FO, Fed. Trust, Central Off., Other: ________ _
Department of Environment, Health, and Natural Resources
DIVISION OF ENVIRONMENTAL MANAGEMENT -GROUNDWATER SECTION /;
0
Lab Number.; fc.1/J>"--"6'-'--rl.,~?=--.,9~------
Date Received ~10/ '70Time -~--'--''53'-"""=c:
Rec'd by: ~ From: Bus, Courier----===----
Other: ________________ _
Data Entry By: ______ Ck: ______ _
Date Reported: _____________ _
Shipped by: Bus, ouri r, Hand Del., Other_· ___________ _
Collector(s): _0.1LS,d:>..~'.',.__-Date '-f,/1/f<, Purpose:,,,,.---......_
Baseline/<:omplaint! Compliance, LUST, Peslicida Study, Federal Trust, Other: _______ _ Time 13.'15
FIELD ANA~'l'.:ES '-ft r,-'
pH400 f"--~--S Spec. Cond.94 ___ at-25" C
Temp.10 , -0 c Odor __ -____ _
Appearance < ( "-s e 1~<.< (,-4d
Field Analysis By: __ l)_"'r ~c~)~,("~""'---------
1 L ~ 1c11cleol'l6)
Owner ire. .--j {-n, ,.,_. I
Location or site 1Jt3 l{;.._fc,/q (?d_ .Cv<--LCt C, •
Description of sampling point 1/ 'J ,-< c~ W<.il 1,c;, >"--
Sampling Meth~d ___ f'_---_--1g;;::"=m+,-,-,.-, .• -"-) ________ Sample Interval, ________ _
Remarks Let .,.,.__,,.._ ,s &t-
lpumping lime, ail 111mp. elc.)
LABORA TORY ANALYSES
BOD. 310 mo/I Diss. Solids 70300 mn'I Ao • Silver 46566 uail Orqanochlorine Pesticides
COD High 340 mg/I Flouride 951 mail Al • Aluminum 46557 ua/I Organophosphorus Pesticides
COD Low 335 mq/I Hardness: Total 900 mail As -Arsenic 46551 ua/1 Nitroaen Pesticides
Coliform: MF Fecal 31616 /100ml Hardness lnon-carb\ 902 ma/I Ba • Barium 46558 uq/I
Coliform: MF Total 31504 /100ml Phenols 32730 un/1 Ca -Calcium 46552 mail Acid Herbicides
TOC 680 mq/I Sgecific Cond. 95 uMhos/cm2 Cd. Cadmium 46559 un/I
Turbidity 76 NTU Sulfate 945 mnil Cr. Chromium 46560 ua/I Semivolatile Organics
Residue., Suspended 530 mg/I Sulfide 745 mail Cu -Conner 46562 ua/I
Fe. Iron 46563 uail
X Ho• Mercury 71900 uotl l:X Volatile Organics (VOA bottle)
pH 403 unit! K -Potassium 46555 mg/I
Alkalinity to pH 4.5 410 mg/I Ma -Maanesium 46554 mat) TPH • Gasoline Range
Alkalinity 1o pH 8.3 415 mg/I Mn -Manqanese 46565 uatl TPH · BTEX Gasoline Range
Carbonate 445 mgtl NH as N 610 mail Na -Sodium 46556 mq/I /
Bicarbonate 440 ma/I I TKN '"N '25 rwll-Ni -Nickel ug/1 I
Carbon dioxide 405 mg/I '-./ NO + NOa as N 630 ma/I Pb · Lead 46564 un/I ..,.
Chloride 940 mg/I P: Total as P 665 mg/I Se . Selenium urul \
Chromium: Hex 1032 uq/I Zn • Zinc 46567 urul
..,.
Color: True 80 Pt-Co
Cyanide 720 mg/I
GW-54 REV. 6/93 For Dissolved Analysis• submit filtered sample and write "DIS" in block.
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
75-35-4
75-09-2
156-60-5
75.34.3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79-34-5
TOL-
T-
E-
U-
N-
0-
M-
COMMENTS:
WATER
1, 1-Dichloroethene 0.75
Methylene Chloride 10
trans-1,2-Dichloroethene 0.75
1, 1-Dich!oroethane 0.25
2,2-Dichloropropane 0.25
cis-1,2-Dichloroethene 0.25
Chloroform 0.25
Bromochloromethane 0.75
1, 1, 1-Trichloroethane 0.25
1, 1-Dichloropropene 0.25
Carbon Tetrachloride 0.75
1, 2-Dichloroethane 0.25
Trichloroethene 0.25
1 ,2-Dichloropropane 0.25
Bromodic hi oromet ha ne 0.25
Dibromomethane 1
cis-1,3-Dichloropropene 0.25
trans-1,3-Dichloropropene 0.25
1, 1,2-Trichtoroethane 0.25
Tetrachloroethene 0.25
1,3-Dich!oropropane 0.25
Dibromochloromethane 0.75
1,2-Dibromoethane
Chlorobenzene 0.25
1, 1, 1,2-Tetrachloroethane 0.25
Bromoform 0.5
1, 1 ,2,2-Tetrachloroethane 0.75
Target Ouantitation Limit-Subject to
change due to instrument sensitivity
Tentatively tder,tified, not confirmed
Estimated Value
Samples analyzed for this compound but not detected
Sample not analyzed for this compound
Detected below quantitation limit
GC/MS Analysis performed
EHNR/DEM LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 96-18-4 1, 2,3-Trichtoropropane
u 108-86-1 Bromobenzene
u 95-49-8 2-Chlorotoluene
u 106-43-4 4-Chlorotoluene
u 541-73-1 1 ,3-Dichlorobenzene
u 106-46-7 1,4-Dichlorobenzene
u 95-50-1 1,2-Dichlorobenzene
u 96-12-8 1,2-Dibromo-3-Chloropropane
u 120-82-1 1,2.4-Trichlorobenzene
u 87-68-3 11 ex achier o but adi ene
u 87-61-6 1 ,2.3-Trichlorobenzene
u 1634-04-4 Methyl-tert-butyl ether
u 71-43-2 Benzene
u 108-88-3 Toluene
u 100-41-4 Ethyl benzene
u 108-38-3 m,p-Xylenes
u 95-47-6 a-Xylene
u 100-42-5 Styrene
u 9B-B2-8 lsopropylbenzene
u 103-65-1 n-Propylbenzene
u 108-67-8-1,3,5-Trimethylbenzene
u 98-06-6 tert-Butylbenzene
u 95-63-6 1,2.4-Trimethylbenzene
u 135-98-8 sec-Butylbenzene
u 99-87-6 p-isopropyltoluene
u 104-51-8 n-Butylbenzene
u 91-20-3 Naphthalene
Other purgeables detected
(up to 1 0 highest peakSJ
NO VOLATILE ORGANIC COMPOUNDS
DETECTED BY GC/ELCD/PID.
LAB NO. 6G669
SUPERVISOR "'&'.?.~
DATE///13
ENTERED BY '/J;J1i
DATE'-f ~':._-(11(,-,
0.25
0.25
0.25
0.25
0.25
0.25
1
0.25
0.25
0.75
5
2
mg/L mg/L
0.25
Detected
ug/L
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u u
u
u
u u
u u
u
N
-.. .5~ he 7-a.,.J,t Se-rv1ce,
.----···-·'-· -----------'----------+------'---------------------------, CII ~r'M~ment of En~r~~~~nt, ~e~I~:, ~~~ ~aturel Resources .
GROUNDWATER FIELD/LAB FORM CHAIN OF '-6M 1Mhl:1NVIRONMENTAL MANAGEMENT. GROUNDWATER SECTION
County 80\Qcl,r,[Q....
Quad No U.o '1,.,,
Lat. 35° L/J' 51/ 11
Serial No. ______ _
Long. 80° 5? 1 6lf 11 rv, D Rec'd by:-"--"'="'--rom: Bu-~ Hand Del.,
~ROUTINE EMERGi:NCY Other: ~
SAMPLE PRIORITY O Date Recei TimeJO:9:)
c::'-, . @CHAIN OF CUSTODY. --j-.-s:cJ.'-,,~-----77,,._..._----
Report To: ARO, FRO,~,_RRO, WaRO, WiRO, Data Entry By:~1--~-~-,--,c==--Ck:-='~/~----
WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported: ~ j /5 /9 5
Shipped by: Bus~ Hand Del., Other· 9'"'t' 1 "-" -ti 4 •111
~u;;r --------. -_----Purpc,se: ..,.. =·. . '-'~ .. ...,
Collector{s): K('onrUCl Date I0l10j95 Time /,) i(Opm Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other· f/pll.t.dv,, flc><.Ju,,o.<;,
" . D. -/ ' ,welo,M) C u
FIELD ANALYSES Owner u(Wid.so,, ''-'-" rt..R_ /.u:,JJ_,,,_ vcw, d,,:w--r, Roc«::1..,, C"
pH400 ---'V!~•u_· __ Spec. Cond.94
1/Dv.'11,os at~ c Location or site I "13 da.LVlt/h /J,1..U.,.<~,,
Temp.10 ~Q~.3~--0c Odor ~v~l=l~'!l..f~---Description of sampling point ~'1.IJ-1:.=~' ~b-i.~·=hl=1 ~C"n-~l){=·=Af=~C9fb,,_t--'L=CU.~~--------------
Appearance Sampling Method ~t?~u..c'-m-'-",p>-------,,====----,,----Sample lnterval-"l-l_'-..ck.-=--'-. ____ _
I Q.' (I~ ) (Pump, bailer. o1c.) .,. / O •
Field Analysis By::$COnnQ c Remarks v.,_r•(\ Cl· c ~ m1,1
LA BORA TORY ANALYSES 1 1 LI a.t l<.C.0fi Cc, ,mpia, tim,. ·'"•mp '"-) o\-<. incl 1/1{1(1AUI
BOD. 310 mQ/1 Diss. Solids 70300 mnil Aa -Silver 46566 uq,I Oraanochlr:1rin6 f)gs!iddu:
COD High 340 mg/I Flouride 951 mQ/1 Al -Aluminum 46557 LIQ/I Organophosphorus Pesticides
COD Low 335 mg/I Hardness: Total 900 maJI As -Arsenic 46551 ua/1 Nitroqen Pesticides
Coliform: MF Fecal 31616 1100ml Hardness (non-carb) 902 mall Ba -Barium 46558 · uall c:
Coliform: MF Total 31504 /100ml Phenols 32730 Unil Ca -Calcium 46552 mall Acid Herbicides '; ·;: _., --
TOG 680 mgn Saecific Cond. 95 uMhos/cm2 Cd -Cadmium 46559 unA ---~· _.., •.. r,! ;-·:-:
Turbidity 76 NTU Sullate 945 mall Cr -Chromium 46560 uall Semivolatile Organics\~~: · ... ,.,
!_ • .' ~ T~
Residue., Suspended 530 mg/I Sullide 745 mn/1 Cu -Coooer 46562 ugll :-·,) ·-·. --.
Fe -Iron 46563 uan ·--' ,, __ . -
X Ha. Mercurv 71900 <.fl. 7 Uall 'X Volatile Organics (VOA b!>ttle) _:: ,,
pH 403 units K -Potassium 46555 mg/I .I ~-.:~·.(:
Alkalinity to pH 4.5 410 mg/I Mo -Maonesium 46554 mail TPH -Gasoline Range :_ --: I)
Alkalinily to pH 8.3 415 mg/I Mn -Manqanese 46565 ug/1 TPH · BTEX Gasoline Range '.~;
Carbonate 445 mg/I NH. as N 610 L'O. 0 I mnll Na -Sodium 46556 mq/1
Bicarbonate 440 mg/I .lliJ'lasJ'L62S mnn Ni -Nickel ug/1 --
Carbon dioxide 405 mall X NO + NO, as N 630 /, 'f mall Pb -Lead 46564 unn I /
Chlorido 940 mg/I P: T ot.il as P GG5 mg/I So -Selenium ua~ V
Chromium: Hex 1 0:.J2 ugJ_I__ Zn• Zinc 46567 ug£1_ --------.. --·
Color: True 80 Pt-Co ·-
Cyanido 7?.0 mgll
Lab Comments:-----------------~--------------~---------------------
GW-54 REV For Dissolved Analysis • submit filtered sample and write "DIS" in ~ · "·
EHNR/DEM LABDRATDRY LAB NO. 5G1747
·lifi~
VOLATILE ANALYTICAL REPORT
REPORTED BY SUPERVISOR ~ CHECKED BY
DATE
REVIEWED BY , ENTERED BY
:S
CHECKED BY ,~$'~
SAMPLE TYPE: WATER ANALYSIS RESULTS
75.35.4 1, 1-Dichloroethene 0.75 u 96-18-4 1,2,3-Trichloropropane 0.25 u
75-09-2 Methylene Chloride 10 u 108-136-1 Bromobenzene u
156-60-5 trans-1,2-Dichloroethene 0.75 u 95-49-8 2-Chlorotoluene 0.25 u.
75.34.3 1, 1-Dichloroethane 0.25 u 106-43-4 4-Chlorotoluene 0.25 u
590-20-7 2, 2-Dichloropropane 0.25 u 541-73-1 1, 3-Dichlorobenzene 0.25 u
156-59-4 cis-1,2-Dichloroethene 0.25 u 106-46-7 1,4-Dichlorobenzene 0.25 u
67-66-3 Chloroform 0.25 u 95-50-1 1,2-0ichlorobenzene 0.25 u
74.97.5 Bromochloromethane 0.75 u 96-12-8 1,2-Dibromo-3-Chloropropane u
71-55-6 1, 1, 1-T richloroethane 0.25 u 120-82-1 1,2,4-Trichlorobenzene 0.25 u
563-58-6 1, 1-Dichloropropene 0.25 u 87-68-3 Hexachlorobutadiene 0.25 u
56-23-5 Carbon Tetrachloride 0,75 u 87-61-6 1,2,3-Trichlorobenzene 0.75 u
107-06-2 1,2-Dichloroethane 0.25 u 1634-04-4 Methyl-tert-butyl ether 5 u
·19-01-6 Trichloroethene 0.25 u 71-43-2 Benzene u
78-87-5 1,2-Dichloropropane 0,25 u 108-88-3 Toluene u
75-27-4 Bromodichloromethane 0,25 u 100-41-4 Ethyl benzene u
74-95-3 Dibromornethane 1 u 108-38-3 m,p-Xylenes 2 u
10061-01-5 cis-1,3-Dichloropropene 0,25 u 95-47-6 a-Xylene u
1 0061-02-6 trans-1,3-0ichloropropene 0.25 u 100-42-5 StVrene u
79-00-5 1, 1,2-Trichloroethane 0.25 u 98-82-8 lsopropylbenzene u
127-18-4 Tetrachloroethene 0.25 u 103-65-1 n-Propylbenzene u
142-28-9 1,3-Dichloropropane 0,25 u 108-67-8 1,3,5-Trimethylbenzene u
124A8-1 Dibromochloromethane 0.75 u 98-06-6 tert-Butylbenzene u
106-93-4 1 .~-Dibromoethane u 95-63-6 1,2,4-Trimethylbenzene u
1 08-90-7 Ch!orobenzene 0.25 u 135-98-8 sec-Butylbenzene u
630-20-6 1, 1, 1 ,2-Tetrachloroethane 0.25 u 99-87-6 p-isopropyltolue~e u
75-25-2 Bromoform 0.5 u 104-51-8 n-Butylbenzene u
79-34-5 1, 1 ,2,2-Tetrachloroethane 0.75 u 91-20-3 Naphthalene u
TOL-Target Ouantitation Limit-Subject to Other purgeables detected Detected
change due to instrument sensitivity (up to 1 0 highest peaks} ug/L
T-Tentatively Identified, not confirmed
E-Estimated Valuo NO VOLATILE ORGANIC COMPOUNDS
U-Samplos analyzed for this compound but not detected DETECTED BY GC/ELCD/PID.
N-Sample not analyzed for this compound
0-Detected below quantitation limit
M-GC/MS Ann1ysis performed
COMMENTS: __________________________________________________________
_
GROUNDWATER FIELD/LAB FORM
County J.wde(,(
Quad No L<o'1q-.'.l'--j Serial No.------
35" l..f::, '.')3 '' ·Long. 8D 0 58'0t," Lat. -=-'"--'-'C-C~-
rqA\N OF ,G SAMl5t~ PRIORITY
~ROUTINE □EMERGENCY
~CHAIN OF CUSTODY
Serv1c.e_
North Carolina
Department of Environment, Health1 end Natural Resource9
DIVISION OF ENVIRONMENTAL MANAGEMENT· GROUNDWATER SECTION
Lab Number -~'r.:t2Tr~::LI.L.TA----?"::::::>""'::--
0
Date Rece·
Rec'd by:__._--==--
Other: ----,-._.,.------------
~::: ~:~~::~:'_t?-'--'\'--\t-1..,5'""--ltf--'~aoL'?S_: ..,_~ ____ _
f
Report To: ARO, FRo,Gl RRO, WaRO, WiRO,
WSRO, Kinston F,9,-F!Rl) Trust, Central Off., Other:
Shipped by: Bus,{QQ!lrier, Hand Del., Other_·-----------Purpcse: · (',,vri-e..,cjl ,3~:;i'.), . ·
Collector(s): k Coone I I Date / 0-IO· q5 Time I.): S6 P'1 Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other· Pni l1A-hm l10,11TIJ1 ,,1.0, Ii') L. · 1c1rcl11 000) . _J
FIELD ANALYSES Owner Dlbedsex)) Ren·ul Tc cu lee
pH (o,O Spec Cond l 10 w•1hvs at 2ef° C Location or site l:::1.1.t-o\c~ ·Bea.cl ._~<,v; I I e..
Te,;.,
0
JC 0 c· Odor rLDAf Description of sampling point Jirie hJ-h® ll.', Lt kqad
Appearanc" cA:,i~ Sampling Method t'W--l' ·
Kc n Fl <,, / ...., .I . ( ,mp, ••1.0,0). Field Analysis By: Onn"-e, RemarkswrY\n Qw af,/!A aWrt14}llK?, ::-,v,.,,.,,,-,\ r O • .....___, (pumping nm,, air 111mp. 01c.)
LABORATORY ANALYSES
Sample Interval 5J -TD
BOD. 310 mo~ Diss. Solids 70300 m"" Aa . Silver 46566 ua/I Orqanochlorine Pesticides
COD High 340 mg/I Flouride 951 mnll Al -Aluminum 46557 ua/1 Organophosphorus Pesticides
COD Low335 mg/I Hardness: Total 900 mail As -Arsenic 46551 ua/I Nilroaen Pesticides '
Coliform: MF Fecal 31616 /100ml Hardness tnon-carb' 902 moll Ba -Barium 46558 unit
Coliform: MF Total 31504 /100ml Phenols 32730 U"" Ca -Calcium 46552 mail Acid Herbicides :_.)
TOC 680 mqn Sgecific Cond. 95 uMhos/cm2 Cd -Cadmium 46559 ua/1 0+ -
Turbidity 76 NTU mnn Cr -Chromium 46560 uon Semivolatile Organic$~~ ---_,'
Sulfate 945 ·-•-~;T;
Residue., Suspended 530 mg/I Sulfide 745 mnn Cu -Conner 46562 uqn "'::: .-, .. <F,~ 1 ,--:
Fe -Iron 46563 U(JII '...._\ : . ..: ... _:._
,.>< Ho -Mercurv 71900 /. T°\. ? uo/I X Volatile Organics (VOA bottle)-.::c·
pH 403 units K -Potassium 46555 mq/I .. • .! ! • ' .. . -
Alkalinity to pH 4.5 410 mg/I Mo: Maanesium 46554 ma/I TPH -Gasoline Range .. J : < ' - • -·:·; :.·::
Alkalinity to pH 8.3 415 mg/I Mn -Manaanese 46565 uo/I TPH · BTEX Gasoline !'lange, ,o
..
Carbonate 445 mgll NH. as N 610 o. l.5 mo/I Na . Sodium 46556 mq/I .::,,J ,·~
Bicarbonate 440 mo~ TKN --f..l ,..,..,... mna Ni -Nickel unn
Carbon dioxide 40S mnn "7--NO +NO asN63o.:?.O m"" Pb -Lead 46564 unn
Chloride 940 mg/I P: Total as P 665 mnn Se -Selenium UO~ I ./
Chromium: Hex 1032 ua/I Zn • Zinc 46567 una V
Color: True 80 Pt-Co
Cyanido 720 mg/I
Lab Comments:_-'----------------------------------------------------
GW-54 REV r-_or Dissolved Analysis -submit filtered sample and write "DIS" in 1:-
EHNR/DEM LABDRA TDRY LAB ND. 5G174B
t2 VDLATILE ANALYTICAL REPORT
REPORTED BY
SUPERVISOR i'
CHECKED BY
DATE
REVIEWED BY
ENTERED BY
CHECKED BY V
SAMPLE TYPE: WATER ANALYSIS RESULTS
75.35.4 1 ;1-Dichloroethene 0.75 u 96-18-4 1,2,3-Trichloropropane 0.25 u
75-09-2 Methylene Chloride 10 u 108-86-1 Bro mo benzene u
156-60-5 trans-1,2-Dichloroethene 0.75 u 95-49-8 2-Chlorotoluene 0.25 u
75.34.3 1, 1-Dichloroethane 0.25 u 106-43-4 4-Chlorotoluene 0.25 u
590-20-7 2, 2-Dichloropropane 0.25 u 541-73-1 1, 3-Dichlorobenzene 0.25 u
156-59-4 cis-1,2-Dichloroethene 0.25 u 106-46-7 1,4-Dichlorobenzene 0.25 u
67-66-3 Chloroform 0.25 0.78 T 95-50-1 1,2-Dichlorobenzene 0.25 u
74.97.5 Bromochloromethane 0.75 u 96-12-8 1,2-Dibromo-3-Chloropropane u
71-55-6 1, 1, 1-Trichloroethane 0.25 u 120-82-1 1,2,4-Trichlorobenzene 0.25 u
563-58-6 1, 1-Dichloropropene 0.25 u 87-68-3 Hexachlorobutadiene 0.25 u
56-23-5 Carbon Tetrachloride 0.75 u 87-61-6 1,2,3-Trichlorobenzene 0.75 u
107-06-2 1,2-Dichloroethane 0.25 u 1634-04-4 Methyl-tert-butyl ether 5 u
79-01-6 Trichloroethene 0.25 u 71-43-2 Benzene u
78-B7-5 1,2-Dichloropropane 0.25 u 108-88-3 Toluene u
75-27-4 Bromodichloromethane 0.25 u 100-41-4 Ethyl benzene 1 u
74.95.3 Dibromomethane 1 u 108-38-3 m,p-Xylenes 2 u
10061-01-5 cis-1,3-Dichloropropene 0.25 u 95-47-6 o-Xylene u
10061-02-6 trans-1,3-Dichloropropene 0.25 u 100-42-5 Styrene u
79-00-5 1, 1,2-Trichloroethane 0.25 u 9B-82-8 lsopropylbenzene u
127-18-4 Tetrachloroethene 0.25 u 103-65-1 n-Propylbenzene u
142-2B-9 1 ,3-Dichloropropane 0.25 u 108-67-8 1,3,5-Trimethylbenzene u
124-48-1 Dibromochloromethane 0.75 u 98-06-6 tert-Butylbenzene u
106-93-4 1,2-Dibromoethane 1 u 95-63-6 1,2,4-Trimethylbenzene u
108-90-7 Chl0robenzene 0.25 u 135-98-8 sec-Butylbenzene u
630-20-6 1, 1, 1,2-Tetrachloroethane 0.25 u 99-87-6 p-isopropyltoluene u
75-25-2 Bromoform 0.5 u 104-51-8 n-Butylbeni:ene u
79.34.5 1, 1 ,2,2-T etrachloroethane 0.75 u 91-20-3 Naphthalene u
TOL· Target Ouantitation limit-Subject to Other purgeables detected Detected
change due to instrument sensitivity (up to 10 highest peaks) u9/L
T-Tentatively Identified, not confirmed
E· Estimated Value NO VOLATILE ORGANIC COMPOUNDS
U-Samples analyzed for this compound but not detected DETECTED BY GC/PID.
N-Samplo not analyzed for this compound
D-Detected below quantitation limit
M· GC/MS Analysis performed
COMMENTS:
Nn~th Car<">line Department of Environment, Health,, Natural
Division of Epidwology
~nvironmentel Epidemiology Section
~ 19-no,-; ~ r;1'hc'
7;;rn /L S e-rt/1 e.e.,_,,
Resources ;'{t.lJJVELJ
JUN 07 1995
Drinkin; Weter HelLlth JUak '!vlLluation
General ,----r I fl
_...:,_,0_;_;:;,llh::..;;U__.Cf.__ COUNTY
/.
DATE J7?,} I)/ LABORATORY N1JKaER 5f 3 0) I J&. 3CJ {
( Baud on the ■: ~elytical roault1, this watar ahould be oon~dared 1afe
for no=l uaa;e.
( ) Chemical analysis did not ah°"' any contu.illation. 'lletar 1bould be
res~led if odor or ta1te per ■i ■ts.
( ) The water should not be used for drinking or cooking purposes, avoid
prolonged bathing/showering.
( ) Baaed on these analytical results, this water i1 hi;hly contlllllineted and
should not be u1ed for drinking, cookin; or bethin9/1howerin9.
( ) The 1a::,oretory results are not conclusive, pleue reaample:
PL!.ASE Ih"D!CATE ON LAB SHUT THAT IT IS A Us.AMPLE A.'O PRO'v!DE PREVIOUS
SAMPLE NUY.BER ( S).
(/
For further information, contact Dr. Ken Rudo or Dr. Luanne Williama,
Environmental Epidemiology Section, [phone].
DEHh""R 3891 (5/92)
Enviro~~entel Epide:r~ology Section (Revie~ 5/95)
GROUNDWATER FIELD/LAB FORM
""'LH\111 .
~,tr·H'i~
County __ '.i_r..,e,.....c\_e._\_\ ___________ _
Quad No Uo'1,., -'is
Lat. 35° l{:)' 58 ''
Serial No. ______ _
Long. So· 5-3' 18 I/
Report To: ARO, FRO,@RRO, WaRO, WiRO,
~ut
SAMPLE PRIORITY
~ROUTINE □EMERGENCY
G;)cHAIN OF CUSTODY
WSRO, Kinston FO, Fe<J. Trust, Central OH., Other: ________ _
North Corollno
Dopnrtmcnt of Envlronmont, Hoalth, nnd Natural Rosourco~
DIVISION OF ENVIRONMENTAL MANAGEMENT -GROUNDWATER SECTION
3<-i-).,
0
Lab Number __5_(-,.:.....,, ~~r3{~l-3G~-~-~~-
Date Recei~ 3.J.!1_l1J. ') Time 0. ,.:2_ '::::>
Rec'd by: US From: Bu~land Del,
Other: ~
~,I Data Entry By:_~V=-A ____ Ck ____ _
Date Reported: _l,_'/,_;,_,0~:::, _________ _
Shipped by: Bus, ~Hand Del., Other· ___________ _ Purpose: ·
Collector(s): I-<. W cu''--"--' Date 3 -LD · C\ S Time I-;;,: 3 0 pH Gasoline, Complaint, Compliance( LUST, Pesticide Study, Federal Trust, Other: i'o1l 1--K'-"1.Jlcoih,,,,,;,
c~el• one) _
FIELD ANALYSES Owner l=°\c,:<2nc.e KCLe>SQ..\.I (R\-->onc\o.... Marg':'"' c, '--",..Q. rj 6w ""'--'l~n -'.i,,,-'"-',
at2s0 c Location or site i?,cn,..tc. IL\ 6cx 3S~ ,6-b::\e-suille f\!c_ :Z<1a'7'7
pH400 -=-=-::=-_Spec. Cond.94 C-:
Temp. 10 _____ 0 c Odor _n..o~_I\..JL~~---Description ol sampling point h,J:c-n 1cn S,n l< "P iti't
Appearance _,_,,""'o.r"'-------------
Field Analysis By: ~'rl,,~\,;)Q.J..==~\c.i,,-,.~~-------
Sampling Melhod ~f~L-'"~P-----=-----------Sample lntervaI_-u..,_"1_L£L_ru.r,=-'-~--
r-{Pump, l).a1!o1, •le) .... ~ • \.D
Remarks 5a."-'>\eo, o..-<-+e, nu..,-,._o·,,.,"l . ' "'"'' 0$ , --:.;;
-=---------r-i--\-W,,mpn~ Dm•. air ltmp. olc.) \...l • •• ., ~ C,")r~-.
LA BORA TORY ANALYSES :: ... . .. ,
BOD, 310 mq/I Diss. Solids 70300 ma1I Aa • Silver 46566 uc,1I Oraanochlorine PesticicloS ';.:.'.I::
COD High 340 mg/I Flouride 951 mn/I Al • Aluminum 46557 uc,1I Organophosphorus Pes\lg'des;\ ~~-1
COD Low 335 mg/I Hardness· Total 900 mgtl As -Arsenic 46551 unil Nitroqen Pesticides ---C . --~ ~-
Coliform: MF Fecal 31616 /100ml Hardness fnon-carb) 902 mn/I Ba -Barium 46550 uqll -· :: )._:-;!Tl --, -,·
Coliform: MF Total 3 l 504 1100ml Pheools 32730 ug!I Ca -Calcium 46552 n=II Acid Herbicides (') I '--:-::.•] : .. :;
TOC 680 moll Sgecilic ConQ. 95 uMhoicm: Cd -Cadmium 46559 un/I en (" --·•
Turbidity 76 NTU Cr -Chromium 4656-0 un/I Semivolatile Orqanics
u, (";
Sulfate 945 mall
Residue., Suspended 530 mg/I Sulfide 745 maJI Cu -Conner 46562 un/I
Fe -Iron 46563 ugil
>< Ha • Mercury 71900 5-:? ug/I >< Volatile Organics (VOA botllo)
pH 403 units K -Potassium 46555 mn/I
Alkalinity to pH 4.5 410 mg/I Ma -Maanesium 46554 mcvl TPH • Gasoline Range
Alkalinity to pH 8.3 415 mg/I Mn -Manaanese 46565 ucvl TPH -BTEX Gasoline Ranga
Carbonate 445 . mg/I NH as N 610 o,oq rna/1 Na -Sodium 46556 mq/I . '
Bicarbonate 440 moll TKN :is~ 625 Ni -tfo.~ls~I ug!I { t "
mgll 'i 1-. /.
Carbon dioxide 405 mq/I .:x NO + N00 as N G30 GJ,'-j mg/I Pb -Load 46564 u,yl , .· (, ... .,--:.. ,., '
r.-,,-1--;-1--1----::-:-·--
Chloride 940 mg/I P: Total as P 665 ma.II Se • Selenium ucvl I /'.I/,. )l'-/j • 5·/\ /.
-
Chromium: Hex 1032 . ua/1 Zn -Zinc 46567 unil \ I '////),. / '.:, .. _ ~~ _,
Color: True oo Pt-Co
V .,<~,I'~., iC~,
Cyanide 720 mg/I
-v~
~)p
Lab Comments: -------------------------------------------------------'~?!,,-,71,-
GW-54 REV For Dissolved Analysis• submit filtered samplo and write "DJS" in b
EHNR/DEM LABORATORY Ll\[l NO. 5G30G
VOLATILE ANALYTICAL REPORT lJ1 REPORTED BY k SUPERVISOR
CHECKED BY
DI\TE t;:,r
REVIEWED BY
EIHERED BY
CHECKED BY
SAMPLE TYPE: WATER ANALYSIS RES UL TS
75-35-4 1, 1-Dichloroethene 0.75 u 96-1 B-4 1,2,3-Trichloropropane 0.25 u
75-09-2 Methylene Chloride 10 u 10B-B6-1 Bromobenzene u
156-60-5 trans-1,2-Dichloroethene 0.75 u 95-49-8 2-Chlorotoluene 0.25 u
75'.34-3 1, 1-Dichloroethane 0.25 0.72 106-43-4 4-Chlorotoluene 0.25 u
590-20-7 2, 2-0 ichloropropane 0.25 u 541-73-1 1,3-Dichlorobenzene 0.25 u
156-59-4 cis-1, 2-Dichloroethene 0.25 0.43 106-46-7 1,4-Dichlorobenzene 0.25 O.B7
67-66-3 Chloroform 0.25 u 9 5-50-1 1,2-0ichlorobenzene 0.25 D
74-97-5 Brornochlorome tl1ane 0.75 u 96-12-8 1,2-Dibromo-3-Ch!oropropa11e 1 u
71-55-6 1, 1, 1-T richloroethane 0.25 u 120-82-1 1, 2,4-Trichlorobenzene 0.25 u
563-5B-6 1, 1-Dichloropropene 0.25 u B7-6B-3 Hex achlorobu tadiene 0.25 u
56-23-5 Carbon Tetrachloride 0.75 u 87-61-6 1, 2,3-T richlorobenze'.1e o. 75 u
107-06-2 1,2-Dichloroethane 0.25 u 1634-04-4 Methyl-tert-butyl ether 5 u
79-01-6 Trichloroethene 0.25 0.27 71-43-2 Benzene u
78-B7-5 1,2-Dichloropropane 0.25 u 1 OB-BB-3 Toluene 1 u
75-27-4 Bro rnodichlororne thane 0.25 u 100-41-4 Ethyl benzene 1 u
74-95-3 Dibrornomethane u 1 08-3B-3 rn,p-Xylenes 2 D
10061-01-5 cis-1,3-Dichloropropene 0.25 u 95-47-6 a-Xylene u
1 OOG1-02-6 trans-1, 3-Dichloropropene 0.25 u 1 00-42-5 Styrene u
79-00-5 1, 1, 2-Trichloroe thane 0.25 u 98-B2-B lsopropylbcnzene u
127-1B-4 T etrachloroethene 0.25 u 103-65-1 n-Propylbenzene u
142-28-9 1, 3-0ichloropropane 0.25 u 108-67-B 1,3,5-Trimethylbenzene u
124-48-1 Oibrornochlorornethane 0.75 u 98-06-6 tert-Butylbenzene u
106-93-4 1, 2-Dibrornoethane 1 u 95-63-6 1,2,4-Trirnethylbenzene u
1 OB-90-7 Chlorobenzene 0.25 u 135-9B-B sec-Butylbenzene u
630-20-6 1, 1, 1,2-Tetrachloroethane 0.25 u 99-B7-6 p-isopro pyltolueno u
75-25-2 Bromoform 0.5 u 104-51-B n-Butylbenzene u
79-34-5 1, 1,2,2-Tetrachloroethane 0.75 u 91-20-3 Naphthalene u
TOL-Target Quantitation Limit-Subject to Other purgeables detected Detected
change due to instrument sensitivity (up to 10 highest peaks) lig/L
T-Tentatively Identified, not confirmed
E-Estimated Value FOUR UNIDENTIFIED PEAKS DETECTED
U-Samples analyzed for this compound but not detected BY GC/ELCD.
N-Sample not amilyzed for this compound ONE UNIDENTIFIED PEAK DETECTED
D-Detected below quantitation limit BY GC/PID.
M-GC/MS Analysis performed
COMrl -s,
_N _o r l r, C ll f O I I II n
GROUNDWATER FIELD/LAB FORM :-;;\ \:.i. !. i;J. r:-:,1_r,_·_' D.rp:llr.tri~O~l(Ot~~~·1f'onmont, Hoolth, ond Nnturnl nosourco:,
lt !'t:C\,[ [i(DIV§[PN (,lf:!;tlVIAdNMENTAL MANAGEMENT. GROUNDWATEll SECTION
County J.N.d. ,Qi,
Quad No l,.(!)1 n-fr 7
Lat. ,35° </ o/ 5 6 ''
Serial No. ______ _
Long. qoo 5 '6'
/44 2-z.J Lab Number-~:~'-./ C,.__-<....,._,.,J,--c']_r-'--:i--~-~--
ROUTINE EMERGENCY __......,
-S~A=M=P~L=E~P~R~IO=R-IT~~ 0 Oat~ Received ;i1:-/ ~ "J Time
□ ~ need by: (}::, f-rorn: BUs .. :::ouric~. Hand Del.,
Other:
/.?:::.--., IBJCHAIN OF CUSTODY ---,n-,;---~r,,=~"'"K~---
Report To: ARO, FRO, ~RRO, WaRO, WiRO, Data Enlry Gy:_~~-___ Ck:'f,...,,e;:~LJ_,_ ___ _
WSRO, Kinston FO, Fed. Trust, Central Off., Other:_________ Date Reported:_
7½~0_/_//,,~if _________ _
Sl1ipped by: Bus, ~Hand Del., Other· ____________ _
~ Purpose:
Collector(s):· KJIJa fi<:gA Date 3-In .q:;-Time \ 2: 'j5' fl"' Oaseline, Complaint, Compliance( LUST, PostIc1de Srudy, Fedor al Trust, Other ~ir ,0 ""·' f,,,,J
c~cl• ur,o)
FIELD ANALYSES Owner f\/\e.r-. (Qsco..c\c\on G,u,>c'l' <'IJ.'-·0 :i~'"'
at 25° C Location or site R IH,u:,_ I<-/ /!, 0.1c 3 YT ::> fr, .. +e-;. L'; ' I " rv<. 2... 9 '-" ·7.,
Description ol sampling point _\s,:,.,_·, J.tt'-'-c..h.1.e<-.a'-'-~"=., ~=k.~~S,+-'s·.ccf'-w_ ________________ _
Sampling Method Jp_lA_rl.-c=t"c-----,,=-===--------Sample Interval _______ _
c::_ _ -(;.' (P~,t.a,liar,olc) -
Remarks ~0 \ < c\ a.: +er 'f' U.l'-'cp. n " '5 h; 0 .$
(purnpru;i tm•, u \emp. al~.)
pH400 -~1-o~-_o __ Spec. Cond.94 ,,.--
Temp.10 __..,.... °C Odor ~Y\.,=n-=1.Q. ___ _
Appearance __<,;.&\[\;1£!.L ___________ _
Field Analysis By: L/-'v~W=oJ=lci,=' _______ _
LABORATORY ANALYSES
BOD 310 mQ/1 Diss. Solids 70300 mail Aa -Silver 46566 ua/I Organochlorine Pesticides
COD High 340 mg/I Flouride 951 m()li Al -Aluminum 46557 uo/1 Organophosphorus Po~ticidf~
COD Low 335 mQ/1 Hardnes~· Total 900 rng.!1 As• Arsenic 46551 uo/1 Nitrogen Pesticides Ul ::;~
Coliform: MF Fecal 31616 /100ml Hardness (non-carbl 902 mail Ba -Barium 46558 uq/1 = ~~l ::.......
Coliform: MF Total 31504 1100ml Phenols 32730 ug/I Ca -Calcium 46552 moil . . Acid Herbicides ~J <:.?.~' ~
TOG 680 mail Specific Cond. 95 uMhos/cm 2 Cd• Cadmium 46559 uo/1 '
-:",=.:"
" ". "
--
Turbidity 76 NTU Sulfate 945 moil Cr• Chromium 46560 unn Semivo!atile Oroanics ---'·--
Residue., Suspended 530 mg/I Sulfide 745 mall Cu -Coooer 46562 uq/I . ~~i::::~
Fe -Iron 46563 ug/1 CJ rn ... ;
·-::::;·
X Ho -Mercury 71900 !, I uru1 >< Volatile Organics (VOA-_t[){Jttle)_0. ..
pH 403 units K -Potassium 46555 mq,I J• n
Alkalinity to pH 4.5 410 mg/I Mq -Magnesium 46554 mQ/I TPH • Gasoline Range
Alkalinity to pH 8.3 415 mg/I Mn -Manqanese 46565 uq/1 TPH . BTEX Gasoline Range
Carbonate 445 mg/I NH asN61oO,n1 mail Na -Sodium 46556 ma.ii
Bicarbonate 440 mwl TKt-J :'!S ~ 625 ,Il\llL Nj -NiQk~I ug/I
Carbon dioxide 405 moil X NO. + NO as N 630 I 0, mo/I Pb · Lead 46564 uo/1 //'"~'
Chloride 940 mg/I P: Total as P 665 ma/I Se -Soleniurn uall ' '--l,r..,,
Chromium: Hex 1032 u(jlf Zn -Zinc 46567 un11 \ /i'J . -~, /_; ' ··~. i /"'1,.<='.
I/ ?,';,-. '/"'")' ~
Color: True ao Pt-Co
I ~ Z..1 ! L " ·.
Cyanide 720 mg/I
•//v n /,...., ·,, /1..,-_i,...,
. l,J }-'J
Lab Comments: ----~-------'-------------------------------------------'_9'-11'1" ~-
-------------------------------------------------------------·""'
,-fyr;
GW-54 REV. For Dissolved Analysis~ submit filtered sample and write "DIS" in b"
EHN11/DEM LABOl1ATOl1Y l.J\U NO. 5(1301
~
VOLATILE ANAL YTIC/\l REPOBT 1}:: REPORTED BY
sui 't:nv1son ' I
CHECKED BY
DATE 3 _b'~1
REVIEWED BY
ENTEl1ED BY
CIIECKED □Y
SAMPLE TYPE: WATER ANALYSIS RES UL TS
75-35-4 1, 1-Dichloroethene 0.75 u 96-1 B-4 1, 2, 3-T richloropropane 0.25 u
75-09-2 Methylene Chloride 10 u 10B-86-1 Bromobenzcne u
156-60-5 trans-1.2·Dichloroethene 0.75 u 95-49-B 2-Chlorotoluene 0.25 u
75:34.3 1, 1 -Dichloroethane 0.25 1.5 106-43-4 4-Chlorotoluene 0.25 u
590-20-7 2, 2-Dichloropropane 0.25 u 541-73-1 1,3-Dichlorobenzene 0.25 u
1 56-59-4 cis-1, 2-0ichloroethene 0.25 3.5 106-46-7 1,4-Dichlorobenzene 0.25 0.27
67-66-3 Chloroform 0.25 OT 95-50-1 1,2-0ichlorobenzene 0.25 u
74-97-5 Bro mochlorornethane 0.75 u 96-12-8 1,2-Dibromo-3-Chloropropane 1 u
71-55-6 1, 1, 1-Trichloroethane D.25 u 120-82-1 1,2,4-Trichlorobenzene 0.25 u
563-58-6 1, 1-Dichloropropene 0.25 u 87-68-3 Hexachloro bu tad ie11e 0.25 u
56-23-5 Carbon Tetrachloride 0.75 u 87-61-6 1,2,3-Trichlorobenzene 0. 75 u
107-06-2 1,2-Dichloroethane 0.25 u 1634-04-4 Methyl-tert-buty! ether 5 u
79-01-6 Trichloroethene 0.25 D 71-43-2 Benzene u
78-87-5 1,2-Dichloropropane D.25 u 1 D8-88-3 Toluene 1 u
75-27-4 Bromodichloromethane 0.25 u 100-41-4 Ethyl benzene 1 u
74-95-3 Dibromomethane 1 u 108-38-3 rn,p-Xylenes 2 u
10061-01-5 cis-1, 3-Dichloropropene 0.25 u 95-47-6 o-Xy!ene u
1 0061-02-6 trans-1,3-0ichloropropene 0.25 u 100-42-5 Styrene u
79-00-5 1, 1,2-Trichloroethane 0.25 u 98-82-8 lsopropylbenzene u
127-18-4 Tetrachloroethene D.25 u 1 D3-65-1 n-Propylbenzene u
142-28-9 1, 3-Dichloropropane 0.25 u 108-67-8 1,3, 5-Trimethylbenzene u
124-48-1 Oibrornochloromethane 0.75 u 98-06-6 tert-Butylbenzene u
106-93-4 1, 2-Dibrornoethane u 95,63-6 1, 2.4-Trimetllylbenzenc u
108-90-7 Ch!orobenzene 0.25 u 135-98-8 sec-Butylbenzene u
630-20-6 1, 1, 1,2-Tetrachloroethane 0.25 u 99-87-6 p-iso pro pyltolue ne u
75-25-2 Bromoform 0.5 u 104-51-8 n-Butylbenzene u
79-34-5 1, 1,2,2-Tetrachloroethane 0.75 u 91-2D-3 Naphthalene u
TQL-Target Quantitation Limit-Subject to Other purgeables detected Detected
change due to instrument sensitivity (up to 1 0 highest peaks) l1g/L
T-Tentatively Identified, not confirmed
E-Estimated Value ONE UNIDENTIFIED PEAK
U-Samples analyzed fClr this compound but not detected DETECTED BY GC/ELCD.
N-Sample not analyzed for this compound ONE UNIDENTIFIED PEAK
D-Detected below quantitation limit DETECTED BY GC/PID.
M-GC/MS Analysis performed
COM~--s,
t
North Corollno
GROUNDWATER FIELD/LAB FORM ,.;·er, H,. \ :,)c (a C D!iPiir;\ri:(•i:itroMii~1fonmont, Health, and Natural Resources
\iff:i ~t [!'(DIVJ§[PN Qf:!;NYIRdNMENTAL MANAGEMENT· GROUNDWATER SECTION
County J.wi e//1,
Quad No L/.D1 Y1 -f4 7 Serial_ No. _____ _
Lat. 35° '-j a-/ 58 ,, Long. _'2'~0~0_5,c....,13~'~1 t./.,__'.c...: __
3'-1-z..
Report To: ARO, FRO, ~ARO, WaRO, WiRO,
WSRO, Kinston FO, Fed. Trust, Central Ott., Other: ________ _
SAMPLE PRIORIT
□ROUTINE ~EMERGENCY
IB'JCHAIN OF CUSTODY 0
Shipped by: Bus, ~ Hand Del., Other_·-'~----------~ Purpose:
Collector(s): KJiJalk;&, Date ..3-<o .q::, Time I 2: '::lS: oh Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other: Po11ut, "" """' l,,,i":J
l \Clftl• ona)
FIELD_ANALYSES Owner A/\Ln Cctscc~ddo.~ C,v-:r,,_-,, 14~1.-s.,--,cn,
at 250 c Location or site R 0-<,.J:,.., 14 /1.c.>c 3 s '1 ~+.tt-e<>L' i I I e ~ 2.. 2"' 'l '7
Description of sampling point Is-, 1-c.-h<-o "', ~ic. '.$ p 190+ pH"°° lo , o Spec. Cond .94 ,,---;
0 c Odor ~~===----Temp.10 .-
Appearance_e.Qii,_,.,_Cl/\,,=-----------
Field Analysis By: ,._)yW=_..,rt.,.Q_,,1@=-~------
LABORA TORY ANALYSES
Sampling Method ~f~lA._n.---c=I",---_· ----,,,=-==,.--------Sample Interval _______ _
c (;' 1Pui:op, ti.1\er. t1c.)
Remarks .;;>"-"'p}"3 C1!o +er f'LLM.f·,n,:i " SM; r,S
tpumpl"li';j llm•, ar ltmp. 11\c.)
BOD 310 ·mail Diss. Solids 70300 mnll AQ -Silver 46566 uQ/I Oraanochlorine Pesticides
COD High 340 mg/I Flouride 951 mo/i Al -Aluminum 46557 ua/1 Organophosphorus Pe~ticidf.~
COD Low 335 mwl Hardness: Total 900 mg/I As• Arsenic 46551 uOII Nitrogen Pesticides U1 :;::
Coliform: MF Fecal 31616 /100ml Hardness (non-carb\ 902 mo/I Ba • Barium 46558 uo/I ~ ..,.v _·,..rr.
Coliform: MF Total 31504 /100ml Phenols 32730 u~'I Ca -Calcium 46552 ='I Acid Herbicides ;;o orT~
TOC 680 m<VI Cd -Cadmium 46559 uo/I -;;:.<
Sgecific ConQ. 9~ uMhos/cm2 -.
Turbidity 76 NTU Sulfate 945 mn1I Cr -Chromium 46560 unn Semivolatile Organics -:--. ,cc,:.._.,
Residue., Suspended 530 mg/1 . Sullide 745 mnn Cu • Conner 46562 uo/I ::r:: J?:~1
Fe• Iron 46563 uo/1 a:> ~~
X Hg -Mercury 71900 /, I ug/I X Volatile Organics (VOA-.l•ottle)n
,_
pH 403 unit~ K -Potassium 46555 mat ,.., ' C
.
Alkalinity to pH 4.5 410 mg/1 Mo • Maonesium 46554 moil TPH -Gasoline Range
Alkalinity to pH 8.3 415 mg/1 Mn . Manqanese 46565 u(lll TPH -BTEX Gasoline Range
Carbonate 445 ' mg/I NH asN61o0,01 m<VI Na . Sodium 46556 mg/I
Bicarbonate 440 m<VI TKN 00 N MC mo/I Ni -Nickol unll
Carbon dioxide 405 mall X NO + NO as N 630 10, moil Pb -Lead 46564 unl1 ff;{ -
Chloride 940 mg/1 P: Total as P 665 mall_ Se . Selenium unn ' , ,~i~.
Chromium: Hex 1032 Uo/1 Zn -Zinc 46567 u(lll \ In /4./,0r, ··~; J/L"
Color: True so Pt-Co \/ '·(//)', ., I ' '-/ !
Cyanide 720 mg/1
'"'14'. / ,
/1~ /On ...
• /~,I . v
Lab Comments: ---~~-------------------------------------------?-,-~'-'1-crr---:P.
GW-54 REV .. For Dissolved Analysis~ submit filtered sample and write "DIS" in b.
EHNR/DEM LABORATORY LAB NO. 5G307
~ VOLATILE ANALYTICAL REPORT
·~
REPORTED BY SUPERVISOR
CHECKED BY DATE -g, ~
REVIEWED BY ENTERED BY
CHECKED BY
SAMPLE TYPE: WATER ANALYSIS RESULTS
75-35-4 1, 1-Dichloroethene 0.75 u 96-18-4 1,2,3-Trichloropropane 0.25 u
75-09-2 Methylene Chloride 10 u 1 08-86-1 Bro mo benzene u
156-60-5 trans-1,2-Dichloroethene 0.75 u 95-49-B 2-Chlorotoluene 0.25 u
75'34-3 1, 1-Dich!oroethane 0.25 1.5 106-43-4 4-Chlorotoluene 0.25 u
590-20-7 2, 2-Dich!oropro pane 0.25 u 541-73-1 1,3-Dichlorobenzene 0.25 u
156-59-4 cis-1,2-Dichloroethene 0.25 3.5 1 06-46-7 1 ,4-Dichlorobenzcne 0.25 0.27
67-66-3 Chloroform 0.25 DT 95-50-1 1,2-Dichlorobenzene 0.25 u
74-97-5 Brornochloromethane 0.75 u 96-12-B 1,2-Dibromo-3-Chloropropane 1 u
71-55-6 1, 1, 1-Trichloroethane 0.25 u 120-82-1 1,2,4-Trichlorobenzene 0.25 u
563-58-6 1, 1 -Dichloropropene 0.25 u 87-68-3 Hexachlorobutadiene 0.25 u
56-23-5 Carbon Tetrachloride 0.75 u 87-61-6 1,2,3-Trichlorobenzene 0.75 u
107-06-2 1,2-Dichloroethane 0.25 u 1634-04-4 Methyl-tert-butyl ether 5 u
79-01-6 Trichloroethene 0.25 D 71-43-2 Benzene u
78-87-5 1,2-Dichloropropane 0.25 u 108-88-3 Toluene u
75-27-4 Bromodichloromethane 0.25 u 100-41-4 Ethyl benzene u
74-95-3 Dibromomethane u 108-38-3 m,p-Xylenes 2 u
10061-01-5 cis-1, 3-Dichloropropene 0.25 u 95-47-6 o-Xylene u
10061-02-6 trans-1,3-Dichloropropene 0.25 u 100-42-5 Styrene u
79-00-5 1, 1,2-Trichloroethane 0.25 u 98-82-B lsopropylbenzene u
127-18-4 Tetrachloroethene 0.25 u 103-65-1 n-Propylbenzene u
142-28-9 1,3-Dichloropropane 0.25 u 108-67-B 1,3,5-Trimethylbenzene u
124-48-1 Dibromochloromethane 0.75 u 98-06-6 tert-Butylbenzene u
106-93-4 1,2-Dibromoethane u 95-63-6 1,2,4-Trimethylbenzene u
108-90-7 Chlorobenzene 0.25 u 135-98-8 sec-Butylbenzene u
630-20-6 1, 1, 1,2-Tetrachloroethane ; 0.25 u 99-87-6 p-isopropyltoluene u
75-25-2 Bromoform 0.5 u 1 04-51-B n-Butylbenzene u
79-34-5 1, 1,2, 2-Tetrachloroethane 0.75 u 91-20-3 Naphthalene u
TQL-Target Quantitation Limit-Subject to Other purgeables detected Detected
change due to instrument s:ensftivity (up to 10 highest peaks) ug/L
T-Tentatively Identified, not ~onfirmed
E-Estimated Value ONE UNIDENTIFIED PEAK
U-Samples analyzed t0r this ~ompound but not detected DETECTED BY GC/ELCD.
N-Sample not analyzed for th\s compound ONE UNIDENTIFIED PEAK
D-Detected below quantitatiofl limit DETECTED BY GC/PID.
M-GC/MS Analysis performed:
COM!. ·s:
GROUNDWATER FIELD/LAB FORM
"U·/l I \'I.
•• Iii 1\1
County __ '.t_,_e_c_l_e._1_1 -----------
Quad No Uo'l ,-, -'is
Lat. .35° J./;)' 58 ,,
Serial No.----~--
Long. So· 5-3 't 8 I/
Report To: ARO, FRO,@g)RRO, WaRO, WiRO,
_~ut
SAMPLE PRIORITY
~ROUTINE □EMERGENCY
~CHAIN OF CUSTODY
WSRO, Kinston FO, Fed. Trust, Central Off., Oiher: ________ _
Shipped by: Bus, ~Hand Del., Oiher_· __________ _
North Carolina
Department of Environment, Heaflh, and Natural Resources
DIVISION OF ENVIRONMENTAL MANAGEMENT· GROUNDWATER SECTION ,..,~
· i-'I< ~~ •"2.f'J r :;/f Lab Number -•-:::c''7~-:~-::'_:.A.,7·=;c''-c;'lJ?'-----,,_,.--=--
o DateRecei~ 'J {q") Time 0:;),5
Rec'd by.· US 1From: Bu~and Del.,
Other: Pv-
Data Entry By: y/¥ Ck~----
Date Reported: --'V_/1111,-'(if=----------
Collector(s): I<. W cu h,_<L, Date 3 -LP -C\ S
Purpose:
Time \-;;, ~ 3 O P'"' Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other: l'Qt\v,;Koa ttooilwi.c,
\ClfCI• one)
FIELD ANALYSES Owner \:\ D( en c..e 'K«.,:,Se.\\ ( R\,-,o,-,da.... Mo,:::f::'=' o ...,:, ,.JI. r:) 6w :f.si. '3 ~,.,_ -s;·,,ro,,s
at 25° c Location or site fl, D1.tD-H 6ox 3sc, , 5-b:\:es v; I\ e N<.. 7 '< 1□ ·17
pH.aa \<> ,0 Spec. Cond.94 ,,--:,;.;;.---Description of sampling point ',,,·,h;..k)~n S,n k 5pifjt\::
Temp.10 _____ °C Odor _ruo~~A.JL.=·~---
Appearance_,._,,~Of=------------
Field Analysis By: ~l::'::,~u&-'--==~\CJIA.=,_----'-----
Sampling Method ~P~L'~"'~P-=---,---.====-------Sample lnterval_~L.<JN __ U1._~<VJ"h-.,.,... __
c _ c\ r, · tP~. barla1,•1c) ....._ c . u'.) , ,
LABORA TORY ANALYSES
RemarkS..:,u.N\• 0.._-,--+e, nu.Ko·,,.,£\.~ "'""'oS -n :;:
-t" r \ (pumpr111 bme, •• l•mp. e1c) ,;.a • :,:o
~ e>rn -
BOD. 310 mQ/I Diss. Solids 70300 mn1I Aq -Silver 46566 UQII Organochlorino Pesticide1i ~rr.
COD High 340 mg/I Flouride 951 mnll Al -Aluminum 46557 uQII Organophosphorus Pes)jgdes;:':~ ~
COD Low 335 mall Hardness· Total 900 mn1I As • Arsenic 46551 UOII Nitrocien Pesticides :',;::~
Coliform: MF Fecal 31616 /100ml Hardness fnon-carbl 902 mnn Ba -Barium 46558 unn :::-:: £"\~~
Coliform: MF Total 31504 /100ml Phenols 32730 un• Ca -Calcium 46552 mnll Acid Herbicides r:,.::, ':.D =~~
TOC 680 mQ/1 Specific Cond 95 uMhos/cm2 Cd -Cadmium 46559 UOII U1 (f} . ··•
Turbidity 76 NTU Sulfate 945 mnn Cr -Chromium 46560 unn Semivolatile Oroanics u (")
Residue., Suspended 530 mg/I Sulfide 745 mQ/I Cu -Conner 46562 UQ/I
Fe -Iron 46563 un/1
>< Hg -Mercury 71900 5-:? ug/1 >< Volatile Organics (VOA bottle)
pH 403 unit:: K -Potassium 46555 mg/I
Alkalinity to pH 4.5 410 mg/I Mo -Maonesium 46554 m01I TPH -Gasoline Range
Alkalinity to pH 8.3 415 mg/I Mn -Manqanese 46565 un/1 TPH -BTEX Gasoline Range
Carbonate 445 ' mg/I NH~· as N 610 o,oq mQ/I Na -Sodium 46556 mq/I ✓ •
Bicarbonate 440 ma/I ' I Tl<N :::ic: N ~?.c; -nO N; -••;nkol un" 'IA,-,
Carbon dioxide 405 mg/I X NO + NO as N 630 '1.y ma/I Pb -Lead 46564 unll , ~{,,J'-. h
Chloride 940 mg/I P: Total as P 665 mall_ Se -Selenium UQ/I \ 'j'(/. 'i/-0 ., #'.,(),
Chromium: Hex 1032 ug/1 Zn -Zinc 46567 unll I / ·---(//). / > '-(,/
Color: True BO Pt-Co
V ''rfl. .,.-,_ .,::P-._....,...
Cyanide 720 mg/I
'''/'+>~ V
. '
Lab Comments: _________ c_ ____________________________________
.£...,~>W,,,--,
GW-54 REV. · 1 For Dissolved Analysis -.submit fi!lered sample and write "DIS" in b . ' -~
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
75.35.4
75-09-2
156-60-5
75034.3
590-20-7
156-59-4
67-66-3
74.97.5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
74.95.3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
1 06-93-4
108-90-7
630-20-6
75-25-2
79.34.5
TQL-
T-
E-
U-
N-
D-
M-
COWi ·s:
WATER
1, 1-Dichloroethene 0.75
Methylene Chloride 10
trans-1,2-Dichloroethene 0.75
1, 1-Dichloroethane 0.25
2,2-Dichloropropane 0.25
cis-1, 2-Dichloroethene 0.25
Chloroform 0.25
Bromoch!oromethane 0.75
1, 1, 1-Trichloroethane 0.25
1, 1-Dichloropropene 0.25
Carbon Tetrachloride 0.75
1,2-Dichloroethane 0.25
Trichloroethene 0.25
1,2-Dichloropropane 0.25
Bromodichloromethane 0.25
Dibromomethane 1
cis-1,3-Dichloropropene 0.25
trans-1,3-Dichloropropene 0.25
1, 1,2-Trichloroethane 0.25
Tetrachloroethene 0.25
1,3-Dichloropropane 0.25
Dibromochloromethane 0. 75
1,2-Dibromoethane 1
Chlorobenzene 0.25
1, 1, 1,2-Tetrachloroethane , 0.25
Bromoform 0.5
1, 1,2,2-Tetrachloroethane 0.75
Target Quantitation Limit-Subject to
change due to instrument sensitivity
Tentatively Identified, not confirmed
Estimated Value
Samples analyzed for this compound but not detected
Sample not analyzed for this compound
Detected below quantitation limit
GC/MS Analysis performed
EHNR/DEM LABO RA TORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RES UL TS
u 96-1 B-4 1, 2, 3-Trichloropropane
u 108-86-1 Bromobenzene
u 95-49-8 2-Chlorotoluene
0.72 106-43-4 4-Chlorotoluene
u 541-73-1 1,3-Dichlorobenzene
0.43 106-46-7 1 ,4-Dich!orobenzene
u 95-50-1 1,2-0ich!orobenzene
u 96-12-8 1,2-Dibromo-3-Chloropropane
u 120-82-1 1,2,4-Trichlorobenzene
u 87-68-3 Hexachlorobutadiene
u 87-61-6 1,2,3-Trichlorobenzene
u 1634-04-4 Methyl-tert-butyf ether
0.27 71-43-2 Benzene
u 1 08-88-3 Toluene
u 100-41-4 Ethyl benzene
u 1 08-38-3 m,p-Xylenes
u 95-47-6 a-Xylene
u 100-42-5 Styrene
u 98-82-8 lsopropylbenzene
u 103-65-1 n-Propylbenzene
u 1 08-67-8 1,3,5-Trimethy!benzene
u 98-06-6 tert-Butylbenzene
u· 95-63-6 1,2,4-Trirnethy!benzene
u 135-98-8 sec-Butylbenzene
u 99-87-6 p-isopropyltoluene
u 104-51-8 n-Buty!benzene
u 91-20-3 Naphthalene
Other purgeables detected
(up to 10 highest peaks)
FOUR UNIDENTIFIED PEAKS DETECTED
BY GC/ELCD.
ONE UNIDENTIFIED PEAK DETECTED
BY GC/PID.
LAB NO. 5G306
SUPERVISOR
DATE
ENTERED BY
CHECKED BY
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.75
5
1
2
1
0.87
D
D
Detected
Lig/L
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
GROUNDWATER FIELD/LAB FORM
. '(J( V
Serial No._____ SAMPLE PRIORITY '\;_,"·_'t:).'\\ 0
80~ 5'il' ,, "\\
Long Ola KjROUTINE □EMERGENCY
Report To: ARO, FRO,@RRO, WaRO, WiRO, ~CHAIN OF CUSTODY
WSRO, Kinston FO, Fed. Trust, Central Off., Other: ________ _
County '---½Q d eJ I
Quad No ¼Jo -9
Lat.J:5°'./J/ 57 ''
Date Receiv
Rec'd by:~~~--
Other: -----;---T7'.t-------~r---'T.r-----
Data Entry By: <Jf;,;;,;-cwS ___ _
Date Reported: -~-1--'-'-llu'0~-)?-' _________ _
Shipped by:,Bus,~, Hand Del., Other_· ___________ _
Collector(s): rl-\JJCU 1:0\ Date -3 -(o '. q S
Purpose:
Time I: <X2 9 r1 Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other: Poll«ti,0 ~o a i 1-t,,·,o:;
f-. 1circl• one) ,
FIELD ANALYSES Owner \1 '.!, J;a.u..rucr ~ GwJ,o 34>=> .s:,1,-,,0 ,
Locationorsite 11:>.!'auno,,-d:v,:.u.Q 1,S/::Q.b;;vdle. f\)C 22(,T1
pH400 (q, O Spec. Cond.94 ~ at 25° C
Temp.10 _,.----c-=---°C Odor _r"--OYU _____ _
Appearance~Q_g,=o..r~------------
Field Analysis By: __.k,!,"""..,_)q,.._,2-a..1\,,Clll\=-------
Description of sampling point hos~ l::,·10\:, Oa ::s·,cte afhoilS< o
Sampling Method ?~~U~rt~r-----~~==~-------Sample Interval l,l.Nko-1 eit,,,'h
LABORA TORY ANALYSES
< I _r '-(PIJIT"4l, t>,.,lllr, •te. \ ~ ...
Remarks 0QH..,o <:'Ll O-.io r pLUYnDur,;, "' -_, 1-,..ns.
-=--=--=r-~ (p\Jmping hm•. air t,mp. ,1c.)
. -T"
BOD 310 mnll . Diss. Solids 70300 matl Ao -Silver 46566 uQ/I Organochlorine Pasticicfiis ~~
COD High 340 mg/I Flouride 951 n,g/i_ Al -Aluminum 46557 unil Organophosphorus Pesticides-.::~;
COD Low335 mnll : Hardness· Total 900 mg/I As -Arsenic 46551 ua/I Nitrogen Pesticides ,_ :r:~c:1
Coliform: MF Fecal 31616 /100ml Hardness (non-carb) 902 ma/I Ba -Barium 46558 un!I co p7::;-:: -r, =:··
Coliform: MF Total 31504 /100ml Phenols 32730 unn Ca -Calcium 46552 =•I Acid Herbicides rrt U>
TOC 680 ma/I Specific Con!! 95 uMhos/cm2 Cd -Cadmium 46559 unn ,:;--, n
Turbidity 76 NTU Sulfate 945 mn!I Cr -Chromium 46560 unn Semivolatile Oraanics
Residue., Suspended 530 mg/I . Sulfide 745 mall Cu . Conner 46562 ua/I
Fe -Iron 46563 unn
,< Ho -Mercury 71900 ./ ,-, •• Y uQ/1 >< Volatile Organics (VOA bottle)
pH 403 unit, K -Potassium 46555 ma/I
Alkalinity to pH 4.5 410 mg/I Mq -Maqnesium 46554 mat TPH -Gasoline Range
Alkalinity to pH 8.3 415 mg/I Mn -Manaanese 46565 ugtl TPH -BTEX Gasoline Range
Carbonate 445 ' mgtl ' NH. as N 610 (J n) mnll Na -Sodium 46556 ma/I
Bicarbonate 440 =II TKP\l ~~ P\l ,....,., ~-" Ni -NickAI unll T /4 ,_
Carbon dioxide 405 mg/I r<.. NO + NO as N 630 /, U-moll Pb -Lead 46564 unil •f~J'./;~
Chloride 940 mg/I P: Total as P 665 ma.-'.1_ Se -Selenium unil I J. /..'j..-~) "Yfi)~
Chromium: Hex 1032 uail ' Zn -Zinc 46567 ua/I \/ ✓ /}irt -/> 'V
Color: True BO Pt-Co
V •,'f/)A lfloA
Cyanide 720 mg/I
···•t;,; ~ .. V
'
Lab Comments: ---------~-----------------~------------------------9_:P,.,_,-,,,.•=-,
GW-54 REV.. , For Dissolved Analysis submit liltered sample and write "DIS" in bl
REPORTED BY
CHECKED BY
REVfEWED BY
SAMPLE TYPE:
75-35-4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79-34-5
TQL-
T-
E-
U-
N-
D-
M-
COMl'r'ITS:
WATER
1, 1-Dichloroethene 0.75
Methylene Chloride 10
trans-1,2-Dichloroethene 0.75
1, 1-Dichloroethane 0.25
2,2-Dichloropropane 0.25
cis-1,2-Dichloroethene 0.25
Chloroform 0.25
Bromochloromethane 0.75
1, 1, 1-Trichloroethane 0.25
1, 1-Dichloropropene 0.25
Carbon Tetrachloride 0.75
1,2-Dichloroethane 0.25
Trichloroethene 0.25
1,2-Dichloropropane 0.25
Bromodichloromethane 0.25
Dibromomethane
cis-1,3-Dichloropropene 0.25
trans-1,3-Dichloropropene 0.25
1, 1,2-Trichloroethane 0.25
Tetrachloroethene 0.25
1,3-Dichloropropane 0.25
Dibromoch!oromethane 0.75
1,2-Dibromoethane 1
Chlorobenzene 0.25
1, 1, 1,2-Tetrachloroethane 0.25
Bromoform 0.5
1, 1,2,2-Tetrachtoroethane 0.75
Target Quantitation Limit-S:Jbject to
change due to instrument sE!nsitivity
Tentatively Identified, not confirmed
Estimated Value
Samples analyzed for this compound but not detected
Sample not analyzed for thi~ co.mpound
Detected below quantitation limit
GC/MS·Analysis performed.
EHNR/DEM LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 96-18-4 1, 2, 3-Trichloropropane
u 108-86-1 Bromobenzene
u 95-49-8 2-Chlorotoluene
u 106-43-4 4-Chlorotoluene
u 541-73-1 1,3-Dichlorobenzene
u 106-46-7 1,4-Dichlorobenzene
u 95-50-1 1,2-Dichlorobenzene
u 96-12-8 1,2-Dibromo-3-Chloropropane
u 120-82-1 1,2,4-Trichlorobenzene
u 87-68-3 Hexachlorobutadiene
u 87-61-6 1,2,3-Trichlorobenzene
u 1634-04-4 Methyl-tert-butyl ether
u 71-43-2 Benzene
u 108-88-3 Toluene
u 100-41-4 Ethyl benzene
u 108-38-3 m,p-Xylenes
u 95-47-6 o-Xylene
u 100-42-5 Styrene
u 98-82-8 lsopropylbenzene
u 103-65-1 n-Propylbenzene
u 108-57-8 1,3,5-Trimethylbenzene
u 98-06-6 tert-Butylbenzene
u 95-63-6 1,2,4-T rimethylbenzene
u 135-98-8 sec-Butylbenzene
u 99-87-6 p-isopropylto luene
u 104-51-8 n-Butylbenzene
u 91-20-3 Naphthalene
Other purgeables detectE!d
(up to 10 highest peaks)
NO VOLATILE ORGANIC COMPOUNDS
DETECTED BY GC/ELCD/PID.
'
LAB NO. 6G308
SUPERVISOR
DATE
ENTERED BY
CHECKED BY
0.25
0.25
0.25
0.25
0.25
0.25
1
0.25
0.25
0.75
5
2
Detected
ug/L
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
GROUNDWATER FIELD/LAB FORM
C OU n ty ~ c:lLlf
Quad No L(p1 m Serial No.----~--
Lat, _______ Long.-----~--
Report To: ARO, FRc@, RAO, WaRO, WiRO,
~ROUTINE □EMERGENCY
~CHAIN OF CUSTODY
WSRO, Kinston FO, Fed. Trust, Central Off., Other: ________ _
N o rt h , C,a i,o I I n a
Department of Envlr~r:tr:ne~'t;\~~e.1th1 and Natural Resources
DIVISION OF ENVIR<:>~MEr,IT~VfflNAGEMENT-GROUNDWATER SECTION
,. '' -' . '
Shipped by: ,Bus,~, Hand Del., Other_· ___________ _
Collector(s): K.vJ03-la,, Date 3 -<o -q 5
Purpose: ·
Time I~\ '5 r"' Baseline, Complaint, Compliancer,k~~JI, Pesticide Study, Federal Trust, Other: foll1dica ttoa·, lw>,g
FIELD ANALYSES Owner I~ '-1 .;ea_LL'Wh ~ 6wiv<. 3~Ja
pH400 lo ,D Spec. Cond.94 ~ at 25° C
Temp.10 --~,--□c Odor_f'-CJNJ._=~---
Appearance _ _,_.""-'"-'-c,---------'----
Field Analysis By: 4l1W=~n.1~1Ch~--------
LABORA TORY ANALYSES
Location_ or site lo1~\ ¾H <De;~~ 1'~1~1;!Q: ~ N,C-, ;;} 'il (Ql"\'1 (;s;'.\"0 r>'.s)
Description ol sampling point"'P~'n _____ )}._ k.o-'-4&-
Sampling Method Polh\:> Sample Interval w\.k.n cr-u)..._,
.C _ ~ 1P~~1lllilr, •le.) ~ ,
Remarks vG4'.C'p led o '{jOLi nlC•m ⇒. ':l ~ (Y\,yl,O,
F (pu l'l\1bm•,nt•mp.etc.)
BOD. 310 mail Diss. Solids 70300 mnll Aa -Silver 46566 unil Organochlorine Pesticides
COD High 340 mg/I Flouride 95 t ma/: Al -Aluminum 46557 Ua/I Organophosphorus Pesticides
COD Low 335 mail Hardness· Total 900 mg'I As -Arsenic 46551 ua/I NitroQen Pesticides
Coliform: MF Fecal 31616 /100ml Hardness lnon-carbl 902 mnll Ba -Barium 46558 ua/I
Coliform: MF Total 31504 1100ml Phenols 32730 ua/I Ca -Calcium 46552 ma/I Acid Herbicides
TOC 680 mg/I Soecific Cond. 95 uMhocJcm1 Cd -Cadmium 46559 · unll
T urbidiJy 76 NTU Sulfate 945 ma/I Cr . Chromium 46560 ua/1 Semivolatile Oroanics
Residua., Suspended 530 mg/I Sulfide 745 mail Cu -Coooer 46562 ug/I \.Cl !..!! -
Fe • Iron 46563 ug/1 ""' -
>< Hg -Mercurv 71900 < o,;;;z ug/I X Volatile Organics (VQ'-bottlej2!
pH 403 units K -Potassium 46555 mail -CP;
Alkalinity to pH 4.5 410 mg/I Mo -Maonesium 46554 mnl TPH -Gasoline Range . --C:Jr,1
Alkalinity to pH 8.3 415 mg/I Mn • Manoanese 46565 ua/I TPH . BTEX Gasolin~ Rari§a--;::
Carbonate 445 ' mg/I NH as N 610 ma/I Na • Sodium 46556 mg/I
----=..,:'I -·=r::
Bicarbonate 440 mnl1 I TKN,. N co, mn,I "1;. "1i~L,, unll .. ;;::,;.<-;:-
Carbon dioxide 405 mnl1 mnll Pb -Lead 46564 unll ,.-r-A ::., ' _(f)
,.~, NO +NO as N 630 , . .h "i":i
-.~ '!Jj.' (~
Chloride 940 mg/I P: Total as P 665 ma/I_ Se• Selenium ua/I
Chromium: Hex 1032 ua/1 Zn• Zinc 46567 ua/1 ., // I);/ ''f y,;;.'
Color: True 80 Pt-Co
. '.f/11, II' I~ '-(/
Cyanide 720 mg/I
·. •1,1t/l~ , .1j7o..,,
.. ,,: V
Lab Comments: ______________________________________________ r-_l,l~=------
,?.
GW-54 REV. For Dissolved Analysis 7 submit filtered sample and wrile "DIS" in bl
" ,_
EHNR/DEM LABORATORY LAB NO. 50309
c&&.
VOLATILE ANALYTICAL REPORT ]ts-REPORTED BY SUPERVISOR
CHECKED BY DATE
REVIEWED BY «'-'<<7~ ENTERED BY
CHECKED BY
SAMPLE TYPE: WATER ANALYSIS RESULTS
75-35-4 1, 1-Dichloroethene 0.75 u 96-18-4 1,2,3-T richloropropane 0.25 u
75-09-2 Methylene Chloride 10 u 108-86-1 Bromobenzene u
156-60-5 trans-1,2-Dichloroethene 0.75 u 95-49-8 2-Chlorotoluene 0.25 u
75-34-3 1, 1-Dichloroethane 0.25 u 106-43-4 4-Chlorotoluene 0.25 u
590-20-7 2, 2-Dichloropropane 0.25 u 541-73-1 1,3-Dichlorobenzene 0.25 u
156-59-4 cis-1,2-Dich!oroethene 0.25 u 106-46-7 1,4-Dich!orobenzene 0.25 u
67-66-3 Chloroform 0.25 u 95-50-1 1,2-Dichlorobenzene 0.25 u
74-97-5 Brompchloromethane 0.75 u 96-12-8 1,2-Dibromo-3-Chloropropane u
71-55-6 1, 1, 1-Trichloroethane 0.25 u 120-82-1 1,2,4-Trichlorobenzene 0.25 u
563-58-6 1, 1-Dichloropropene 0.25 u 87-68-3 Hexachlorobutadiene 0.25 u
56-23-5 Carbon Tetrachloride 0.75 u 87-61-6 1,2,3-Trich[orobenzene 0.75 u
107-06-2 1,2-Dichloroethane 0.25 u 1634-04-4 Methyl-tert-butyl ether 5 u
79-01-6 Trichloroethene 0.25 u 71-43-2 Benzene u
78-87-5 1,2-Dichloropropane 0.25 u 108-88-3 Toluene u
75-27-4 Bromodichloromethane 0.25 u 100-41-4 Ethyl benzene u
74-95-3 Dibromomethane u 108-38-3 m,p-Xylenes 2 u
10061-01-5 cis-1,3-Dichloropropene 0.25 u 95-47-6 a-Xylene u
10061-02-6 trans-1,3-Dichloropropene 0.25 u 100-42-5 Styrene u
79-00-5 1, 1,2-Trichloroethane 0.25 u 98-82-8 lsopropylbenzene u
127-18-4 Tetrachloroethene 0.25 u 103-65-1 n-Propylbenzene u
142-28-9 1,3-Dichloropropane 0.25 u 108-67-8 1,3,5-Trimethylbenzene u
124-48-1 Dibromochloromethane 0.75 u 98-06-6 tert-Butylbenzene u
106-93-4 1,2-Dibromoethane u 95-63-6 1,2,4-Trimethylbenzene u
108-90-7 Chlorobenzene 0.25 u 135-98-8 sec-Buty!benzene u
630-20-6 1, 1, 1,2-Tetrachloroethane 0.25 u 99-87-6 p-isopropyltoluene u
75-25-2 Bromoform 0.5 u 104-51-8 n-Butylbenzene u
79-34-5 1, 1,2,2-Tetrachloroethane 0.75 u 91-20-3 Naphthalene u
TQL-Target Quantitation Limit-Subject to Other purgeab!es detected Detected
change due to instrument sensitivity (up to 10 highest peaks) ug/L
T-Tentatively Identified, not confirmed
E-Estimated Value NO VOLATILE ORGANIC COMPOUNDS
U-Samples analyzed for this ~ompound but not detected DETECTED BY GC/ELCD/PID.
N-Sample not analyzed for this_ compound
D-Detected below quantitation limit
M-GC/MS-Analysis performed'
COMl'r"TS:
State of North Carolina
Department of Environment,
Health and Natural Resources
Mooresville Regional Office
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
Linda Diane Long, Regional Manager
DIVISION OF ENVIRONMENTAL MANAGEMENT
January 4, 1995
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
A.A.A. Enterprises, Incorporated
Route 14, Box 350
Statesville, North Carolina 28677
Attention: Barry Dean Sigmon
RE: Final Extension
Dear Mr. Sigmon:
Sigmon Septic Tank Service
Incident N' 3422
Iredell County, North Carolina
On August 9, 1990, you were served a Notice of Violation
(NOV) from the Division of Environmental Management (DEM) for
violation of the North Carolina groundwater standards. In the
NOV you were required to determine the vertical and horizontal
extent of soil and groundwater contamination and to submit a site
assessment report within 60 days of receipt of the NOV. The NOV
was held in abeyance pending a review by the Hazardous Waste
Section of the Division of Solid Waste Management. After the
Hazardous Waste Section concluded that the site did not fall
under its jurisdiction, the DEM reissued a NOV to you on July 13,
1993, which required you to submit a site assessment report
within 60 days of receipt of the NOV.
On December 21, 1993 the DEM issued you a Notice of
Regulatory Requirements for 15A NCAC 2L . 0.1 06 ( f) ( 3) and ( 4) which
required that primary and secondary pollution sources be removed,
treated, or controlled prior to or concurrent with assessment
activities. A schedule was established allowing the lagoons to
be closed in phases with the final lagoons to be closed by July
1, 1994. Per your request, the DEM granted an extension until
November 30, 1994 for the closure of the lagoons. On October 24,
1994, you requested an additional extension as well as a meeting.
After speaking with you on November 22, 1994 the DEM attempted to
contact you by telephone on two separate occasions, but has been
unsuccessful. ·
919 North Main Street, Mooresville, North Carolina 28115 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post-consumer paper
Mr. Barry Dean Sigmon
January 4, 1995
Page Two
. The purpose of this letter is to formally notify you that
uniess documentation that lagoons W 1 through W 7 have been
closed is submitted by no later than 90 days from the date of
your receipt of this letter, this Office will refer the matter to
the Director for enforcement action on the violations of the
groundwater quality standards and for your continuing violation
of 15A NCAC 2L .0106(c). Pursuant to G.S. 143-215.6C, the
Secretary may also seek an injunction requiring you to take
action consistent with the Commission's rules and in accordance
with the cleanup provisions of the Oil Pollution and Hazardous
Substances Control Act. You should note that any enforcement
action, including an assessment of civil penalties, may begin
from the original due date established in the July 13, 1993
Notice.
Should you have any questions, please contact Karen Walker
or me at [phone].
Sincer:ly, /J
~eithO(f;~
Re ional Supervisor
cc: Pollution Incident Branch -Raleigh
KDW/sc
North Carolina
G OUNDWAJER FIELD/LAB FORM Department of Environment, Health, and Natural Resources
R . ~HAIN o F CUSTODY DIVISION OF ENVIRONMENTAL MANAGEMENT. GROUNDWATER SECTION
County I,<
Quad No L"' 'I.-, · 'G Serial No. ______ _
Lab Number 4G /51}'7
SAMPLE PRIORITY Date Received 10/ t8Lq 1 Timeq,ZJZ) ·
-· Rec'd b. y~
1
horn: Bus~Hand Del., □ROUTINE [8EMERGENCY ~
GZlcHAIN OF CUSTODY
0th
er: { /ff. . Ck·.0'0
Lat. _______ Long. ________ _
ReportTo:ARO,FRO@RRO,WaRO,WiRO, ~ DataEntryBy: ::;m._ :~----
Shipped by: Bus Couri~. Hand Del., Other_· ____________ Purpose: G,vJ S,.,._ r;: 3 ~--;:;cs,~1°•'>) .
Collector(s): l::,,l,Vo.J\lQ.L Date ID· ' -.GJ '-l Time 1;;,.'-:::,_ 5 pn Baseline, Complaint, Compliance LUST, Pesticide Study, Fede}~ Trust, Other: Yoll~--ho 0 YI<.>, ,-1-vrir,;
T ( (c1rc!e ono) ..__ ___ . _ _ _ __ ,.,. ../
FIELD ANALYSES Owner I; I ore oc r }s, c<.-,o? 11 +.,.~ ~.~1 ) .. '7::.hc~c{ << n c•,,y-·,{ v.:l .Q. 11 o, ,)rJI .. [
pH400 {,.n Spec.Cond.94 8?0,""I"< atJli""C Locationorsite'J;c,,1£ IL\o , ?,,,,., 30.. Si-.--.i-~sv'-11, --,,.'2 -.,,7
Temp.10 1'-l 0 c Odor """' Description of sampling point 'Tier ,,,,_ccf-, k,,.,, < @ u..J,,.J1
Appearance W !<'. Sampling Method _P_''-"..,Pcc-------===:;-;;;.,---------Sample lnterval~c~c-'~v->~-"~~c_·.-.~-~
Field Analysis By· f<NVJlu,, Remarks ~ ?/eel · r J -1P"':''·"''"'·"'1 :< S n--c•"'-5 _
LABORATORY ANALYSES
BOD. 310 mail Diss. Solids 70300 mall
COD High 340 mg/I Flouride 951 ma/I
COD Low 335 mg/I Hardness: Total 900 mg/I
Colilorm: MF Fecal 31616 1100ml Hardness (non-carb) 902 moil
Coliform: MF Total 31504 1100ml Phenols 32730 un/I
TOC 680 mall Soecific Cond. 95 uMhos/cm2
Turbiditv 76 NTU Sullate 945 ma/I
Residue., Suspended 530 mg/I Sulfide 745 ma/I
pH 403 unit~
Alkalinity to pH 4.5 410 mg/I
Alkalinity to pH 8.3 415 mg/I
Carbonate 445 mg/I NH as N 610 mrul
Bicarbonate 440 mn< TK/\1 ~~-N ~,.,,, ~""
Carbon dioxide 405 mg/I V NO + NO as N 630 'l, '). moil
Chloride 940 mg/I P: Total as P 665 mQ/I
Chromium: Hex 1032 Ua/I
Color: True eo Pt-Co
Cyanide 720 mg/I
GW-54 REV. W"?
'
For Dissolved Analysis• submit filtered sample and write "DIS" in block
I
V
umping 11m,, air temp. etc.) ·---r ill
Ao • Silver 46566 . Ua/1 Organochlorine Pes~es C?, j"T1
Al • Aluminum 46557 Ua/I Organophosphorus R.esticioes;+,
As. Arsenic 46551 ua/1 Nitrogen Pesticides I :;Z -c:::
Ba . Barium 46558 ua/1
_,. _c
Ca • Calcium 46552 ma/I Acid Herbicides :.·.::: 9.rTl
Cd • Cadmium 46559 ua/1 -f'.'T1":,:;; -
Cr• Chromium 46560 U!JII Semivolatile Organics ;;.. --Ul
Cu -Coooer 46562 u~I -0
Fe • Iron 46563 Ug/1
Hq • Mercury 71900 3,;L uq,I V volatile Organics (VOA bottle)
K • Potassium 46555 mg/I
Mo -Maanesium 46554 mg/I TPH • Gascline Range
Mn . Manoanese 46565 Uq;I TPH . BTEX Gasoline Range
Na • Sodium 46556 ma/I
Ni· Nickel Uail
Pb -Lead 46564 ua/1 ?
Se • Selenium ug/I I
Zn• Zinc 46567{ i'-1 . ~-. :< ;; ! C£._ l ua/I I
~ ~~ "•' ,1..~ '.'! it iJ.._ it_J
,ULv Q n ,,.,,. /) I'• ·.·I,
GROUNDWATER FIELD/LAB FOAM
n North Caroline
, USTO r, v o.i-tment o1 e.,.,,,,_,,..,., HoaM, -Natuna1 ~
. ' follllSIOH Of' ENVIRONMENTAL IIANAGEIIEHT-Gfl00NOWAT£R SECTIOH
BOO 310 """ . n. •• _ ""'""' 70300 mnl1 Ao -Silve< 46666 uni! Omanochlorine Pesticides
coo High J.40 mg.1 Flouride 951 mall Al -Alumir,.1m 46557 un/1 Orgaoophosphoruo Pesticideo
COO low 335 m<YI . . T ... 1 .. 1 tv'\n mo'! As• Arsenic 46561 '""' Nitronen Pesticides
Colilofm: MF Fecal 31616 1100ml Hardness (non-carbl 002 =JI y Ba -Barium 46568 S-'7 """ ·-~
Colilofm: MF Total 31~ /100ml nnn '.,,,, Ca• Calcium 46562 mnJ Acid Herbicide• .i;-::i=
TOC 680 mg,1 . -r~n,1 "" ' y C<I • Cadmium 46569 <.,?, 0 '""'
;,:..,: c,;;,;,
Turbidity 76 NTU Sulfate 945 mnl1 Cr -Chrnmium -46560 u<r/1 Semivolafile Oroanica ---0 ci5'>
RndJo., Suspended 530 mg.1 Suttide 745 mn!I >< Cu -Coooer 46562 c;-, 1-f UOII co ::E<
X Fa -Iron 46563 /3DO ug,1 --,, -c:,
>< Hg-Mercurv 71000 <o,;;). ugl1 y VolatiHt Organics (VOA boilll) Pr,,
pH <403 units
K • Potassium 465.55 mn/1 9 ,,,_
-:z:
Alkalinitv 10 pH 4.5 410 mg.1
Ma -Maaneoivm 4656-4 mn~ TPH -Gaaoline Ranoe -.,,-
Alkalinitv 10 pH 8.3 415 mg,1
X Mn -Manganese 46565 3 ,7 U0/1 TPH -BTEX Gaaoline Ranae ... c-,
Carbonate «5 mg.1 -{ NH uN BlO 0, Qj mn!I y Na -Sodum 46556 ,; ;i ma/
Bicarbonall 440 mnl1 Tl(>,I •• IJ ·--J\ \/ "'' -,.,.,.,., I J' '.,,,,
Carbon cioxide 405 mwt y NO +NO asN ""'0, 35 mnl1 v. Pb -lead 46564 < / 0 uo/1
Chkxide 940 . mg/I ' P: Tola! as P 665 mnl1 Se -Selenium UOII . J
Chromium: Hax 1032 UOII '·.' \ '" x Zn • Zinc 46567 <" J 0 un/1 V
Colo<: T I\JO &Cl Pl-Co CCi'l I\ () ,cu1;
Cyanide 120
~--, ,, . '
. mg.1
'
--
Lab Comments: ______________ •n_,_1 _11_11_1!_1,,_r_:'_"·_' ·_ .. _' ,_. _,.,_!!_~_~•-~_-' ____________________________
_
Fn< Dissolved Analysis • submil tih0<ed aample and wiile ·01s· in blocit · ·
~?C~ till SY
CH=C:"\ED5Y
REVIEWED BY
75-35-4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
7 4-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79-34-5
TQL-
T-
E-
U-
N-
D-
M-
COMMENTS:
1, 1-Dichloroethene 0.75
Methylene Chloride 10
trans-1,2-Dichloroethene 0.75
1, 1-Dichloroethane 0.25
2,2-Dichloropropane 0.25
cis-1,2-Dichloroethene 0.25
Chloroform 0.25
Bromochloromethane 0.75
1, 1, 1-Trichloroethane 0.25
1, 1-Dichloropropene 0.25
Carbon Tetrachloride 0.75
1,2-Dichlo"roethane 0.25
Trich!oroethene 0.25
1,2-Dichtoropropane 0.25
Bromodichloromethane 0.25
Oibromoniethane
cis-1,3-Dichloropropene 0.25
trans-1,3-Dichloropropene 0.25
1, 1,2-Trichloroethane 0.25
Tetrachloroethene 0.25
1,3-Dichloropropane 0.25
Oibromochloromethane 0.75
1,2-Dibromoethane
Chlorobenzene 0.25
1, 1, 1,2-Tetrachloroethane 0.25
Bromoform 0.5
1, 1,2,2-Tetrachloroethane 0.75
Target Quantilation Limit-Subject to
change due to instrument sensitivity
Tenta~ively Identified, not confirme_d
Estimated Value
Samples analyzed for this compound but not detected
Sample not analyzed for this compound
Detected below quantitation limit
GC/MS Analysis performed
EHNRIDEM LA BORA TORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 96-18-4 1,2,3-T richloropropane
u 108-86-1 Bromobenzene
u 95-49-8 2-Ch!orotoluene
u 106-43-4 4-Chlorotoluene
u 541-73-1 1,3-Dichlorobenzene
u 106-46-7 1,4-Dichlorobenzene
u 95-50-1 1,2-Dichlorobenzene
u 96-12-8 1, 2-Dibromo-3-Chloropropane
u 120-82-1 1,2,4-Trich!orobenzene
u 87-68-3 Hexachlorobuladiene
u 87-61-6 1,2,3-Trichlorobenzene
u 1634-04-4 Melhyl-lert-bulyl elher
u 71-43-2 Benzene
u 108-88-3 Toluene
u 100-41-4 Ethyl benzene
u 108-38-3 m,p-Xylenes
u 95-47-6 a-Xylene
u 100-42-5 Styrene
u 98-82-8 lsopropylbenzene
u 103-65-1 n-Propylbenzene
u 108-67-8 1,3,5-T rimethylbenzene
u 98-06-6 tert-Butylbenzene
u 95-63-6 1,2,4-Trimethylbenzene
u 135-98-8 sec-Butylbenzene
u 99-87-6 p-isopropyltoluene
u 104-51-8 n-Butylbenzene
u 91-20-3 Naphthalene
Other purgeables detected
(up lo 10 highesl peaks)
NO VOLATILE ORGANIC COMPOUNDS
DETECTED BY GC/ELCD/PID.
LAB NO. 4G11I2
SUPERVISOR
DATE
ENTERED BY
CHECKED BY
0.25
1
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.75
5
2
1
Detected
ug/L
_/
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
State of North Carolina
Department of Environment,
Health and Natural Resources
Mooresville Regional Office
Jomes B. Hunt. Jr .. Governor
Jonathon B. Howes, Secretory
.BA
DEHNA.
DIVISION OF ENVIRONMENTAL MANAGEMENT
September 13, 1994
Ms. Mary L. Sigmon
A.A.A. Enterprises, Incorporated
Route 14, Box 350
Statesville, North Carolina 28677
Dear Ms. Sigmon:
RE: Request for Extension
Sigmon Septic Tank Service
Groundwater Incident W 3422
Iredell county, N.C.
Steven Burrow's request, on your behalf, for additional time
for submitting the documentation that the lagoons have been
properly closed at the above referenced site has been reviewed by
the Groundwater Section of the Mooresville Regional Office.
Based on the information you have provided with your request
for an extension, the request is hereby granted until November 30,
1994. Failure to send the documentation by the extended due date
may result in a recommendation for the assessment of civil
penalties beginning from the original due date.
Should you have further questions regarding this matter,
please call Chris DeRoller or me at [phone].
cc: Incident Management Unit
CMD/sg
Sincerely,
~~1\1)
Brenda J. Smith, P.G.
Regional supervisor
919 North Main Street, Mooresville, North Carolina 28115 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ l 0% post-consumer paper
GROUNDWATER FIELD/LAB FOAM
Seri8I No, _____ _
Long. fiv' 5,9 1'5"
800 310 ""'" ni-~'1n'VV\ mnl1
COO!ti:J40
mo,! Flouriclo 115 t mo,!
COOLowlXI IT1Q/'I . · TN .. nnn mnl1
CoWorm: MF Focal 31611 1100ml Ha,dnoH lnon-carbl °"' mn/1
Colilorm: MF Told 31604 /100m ·'l?nn un.1
TOCaeo
mo,! SQICilic;Cond.l!:i uMhcJ.,rml
T•-7& NTU Sulfate w5 mn/1
l\oclcl>o., s.,,."M<led e.10 mg,1 Su!lide 745 mo,!
pH403
unit,
Allu,linilY to _pH 4.5 •10 roo/1
.. to pH 11.3 •11 ma'I
Carbonalo 445 ma'I y NH uN eto0,0/ ma'I
Bicarbonate 440 mn/1 TIO/•• N -
,....,.
Clllbon dio•ldo 405 mo,! )( M<l + '"" .,. N A"VI O, Oi.f mn11
Chlorid■ IMO 111!)"1 P: fn1.i-p665 mn/1
Clwomiurn: He• 11132 un/1 •,\,fl-. i .. , . 't, / '
Color: True ea Pl-Co ---~ ' ..
Cyanide 720 nv1
.)[r' U '/ i,;4
><
✓-
:,(
y
X
)("
:x
:✓
')(.
y
Norlll Carollno
~-of [nwt,o,-, Hemtft, end Nceural Fie•, ION
OIVISION Of' ENYIRONIW:KTAL MAHAGEIIENT -GIIO(JNDWA lVI 15EC110N
An-Siver-un/1 r ·=-·--:: P1 f :ides
Al· Aluminum .w;M7 ua,1 Orpanophc,11"'101119 PeabcidH
As • A, .. nic .w;M I ua/1 Nilrooon PnlicidH
, 8a -Barium ™69 35 ua/1
C■ -Calcium uu.:, RD Acid HorolddN
Cd· Cadmium .-o <:".:?, 0 ua,1
lO 01
Cr -Clwomium ,4668) ua,1 Somi¥alatile r ----:-
Cu· 46662/-'/ ua,1
~ ;i51'11
Fe-lron,16563 /6 0 ua,1
I ~"1
Hg • Mo,cury 71IIOO <rJ, ;;i__ ua,1 Y, Vole/Ao Ogonl<:s (VOA """"'' c3::::,
K • Pol■asium 465156 mw
:t,,. ~SJ -
Un . I.AaQ,wsium 46664 me/ TPH • Guolinct ---i'-'-'
Mn -Mannaneao 46566 / ;)O ua,1 TPH-BTEXGMoli,..,-.
;:o;z:
Na -Sodum "6556 o?, (o mu,'
r.n ;,:,:
............. < ;,.., unA I ~-"
Pb-l ■ad--C/() uni! \/
Se • Selenium uni!
Zn -Zinc ..-1 / 3D uni!
I
RE.PORTED BY
C~ECKEUEY
REVIE\VEO SY
75-35-4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
563-56-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-26-9
124-46-1
106-93-4
106-90-7
630-20-6
75-25-2
79-34-5
TOL-
T-
E-
U-
N-
D-
M-
COMMENTS:
1, 1-Dichloroethene 0.75
Methylene Chloride 10
trans-1,2-0ichloroethene 0.75
1, 1-Dichloroethane 0.25
2,2-Dichloropropane 0.25
cis-1,2-Dichloroethene 0.25
Chloroform 0.25
Bromochloromethane 0.75
1, 1, 1-Trichloroethane 0.25
1, 1-Dichloropropene 0.25
Carbon Tetrachloride 0.75
1,2-Dichloroethane 0.25
Trichloroethene 0.25
1,2-Dichloropropane 0.25
Bromodichloromethane 0.25
Oibromomethane
cis-1,3-Dichloropropene 0.25
trans-1,3-Dichloropropene 0.25
1, 1,2-Trich_loroethane 0.25
Tetrachforoethene 0.25
1,3-Dichloropropane 0.25
Dibromochloromethane 0.75
1,2-Dibromoethane 1
Ch!orobenzene 0.25
1, 1, 1,2-Tetrachloroethane 0.25
Bromoform 0.5
1, 1,2,2-Tetrachloroethane 0.75
Target Quantitation Limit-Subject to
change due to instrument sensitivity
Tentatively Identified, not confirmed
Estimated Value
Samples analyzed for this compound but not detected
Sample not analyzed for this compound
Detected below quantitation limit
GC/MS Analysis performed
EHNRIDEM LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 96-16-4 1,2,3-Trich!oropropane
u 106-66-1 Bromobenzene
u 95-49-6 2-Chlorotoluene
u 106-43-4 4-Chlorotoluene
u 541-73-1 1, 3-Dichlorobenzene
u 106-46-7 1,4-Dich!orobenzene
u 95-50-1 1,2-Dichlorobenzene
u 96-12-6 1,2-Dibromo-3-Chloropropane
u 120-82-1 1,2,4-Trichlorobenzene
u 67-66-3 Hexachlorobutadiene
u 67-61-6 1,2,3-Trichlorobenzene
u 1634-04-4 Melhyl-tert-butyl ether
u 71-43-2 Benzene
u 106-66-3 Toluene
u 100-41-4 Ethyl benzene
u 106-36-3 m,p-Xylenes
u 95-47-6 o-Xylene
u 100-42-5 Styrene
u 96-62-8 lsopropylbenzene
u 103-65-1 n-Propylbenzene
u 108-67-8 1,3,5-Trimethylbenzene
u 96-06-6 tert-Butylbenzene
u 95-63-6 1,2.4-Trimethylbenzene
u 135-96-6 sec-Butylbenzene
u 99-67-6 p-isopropyltoluene
u 104-51-6 n-Butylbenzene
u 91-20-3 Naphthalene
Other purgeables detected
(up lo 10 highest peaks)
NO VOLATILE ORGAN:C COMPOUNDS
DETECTED BY GC/ELCD/PID.
LAB NO. 4G1113
SUPERVISOR
DATE
ENTERED BY
CHECKED BY
0.25
1
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.75 .
5
1
2
1
1
Detected
ug/L
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
.U
u
u
u
u
u
u
u
State of North Carolina
Department of Environment,
Health and Natural Resources
Mooresville Regional Office
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
Vivian H. Burke, Regional Manager
AVA
DEHNR
DIVISION OF ENVIRONMENTAL MANAGEMENT
June 9, 1994
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
Mary L. Sigmon
A.A.A. Enterprises, Incorporated
Route 14, Box 350
Statesville, North Carolina 28677
Dear Ms. Sigmon:
RE: Request for Extension
Sigmon Septic Tank Service
Groundwater Incident W 3422
Iredell County, N.C.
Steven Burrows' request, on your behalf, for additional time
for submitting the documentation that lagoons. 5, 6 and 7 have been
properly closed at the above referenced site has been reviewed by
the Groundwater Section of the Mooresville Regional Office.
Based on the information you have provided with your request
for an extension, the request is hereby granted until July 1, 1994.
Failure to send the documentation that lagoons 2, 3, 4, 5, 6 and 7
have been properly closed by July 1, 1994 may result in a
recommendation for the assessment of civil penalties beginning from
the original due date.
In addition to the above, in a July 13, 1993 Notice of
Violation you were notified of your responsibility to provide an
alternate drinking water supply for the residents who use the wells
at Route 14, Box 356 and Box 357. It is our understanding that you
are providing bottled water to these residences. Please be advised
that you should be providing a minimum of 2 liters of water per
person per day. Therefore, you should be providing 15 gallons of
water per week to the residence at Box 356. It is my understanding
that there is no one currently living at the residence at Box 357,
so no water is required until a new tenant moves in.
919 North Main Street, Mooresville, North Carolina 28115 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ l 0% post-consumer paper
A.A.A. Enterprises, Incorporated
June 9, 1994
Page Two
Should you have further questions regarding these matters,
please call Chris DeRoller or me at [phone] .
....__j~-V-~,<.,/ ___ _
~r da J. Smith, P.G.
Regional Supervisor
cc: \Incident Management Unit
CMD/sc
~. ,,. ,.,.,
ht.1.i[IVE,:}
JUN 1 0 1994
POLLUIJQN CONTROL BRANCH
. -......
GROUNDWATER FIELD/LAB FORMr,;/i\}~;l\ (~f
-V North Carollna
{'A! i ~~r OD\ Department of Environment, Health, and Natural Re90urces
":..!'\•'-' ll · DIVISION OF ENVIRONMENTAL MANAGEMENT· GROUNDWATER SECTION
County Irec\.e Ii
Quad No I b '1 r1~ >I Serial No.------SAMPLE PRIORITY
Lat. ______ Long.-------LZjROUTINE □EMERGENCY
[gjcHAIN OF CUSTODY
Report To: ARO, FRO@,)RRO, WaRO, WiRO,
WSRO, Kinston FO, Fed. Trust, Central Off., Other: ________ _
Shipped by: Bus, Courier, Hand Del., Other·-,------------
Collector(s): J)c~l\u Date 3 §5/ytf
FIELD ANALYSES
0
Lab Number C--s: ;33::;i._
Date Received 3 ·I {0 ::'1 lJ.. Time £· 3
Rec'd byQS From: B s, Courie Hand Del.,
Other: ---------~--c~-----
Data Entry By: & C~
Date Reported: -~t,_',;l.~64=:<L=. ==---=---c._ __
-rnc1ct:.,,.L~<dv
pH.,., _____ Spec. Cond.94
Temp.10
°c Odor _____ _ Description of sampling point --'"-""''f"---''-''-'-k"','-. '-1-'-cl.-'-c"-''-'"--------------------
Sampling Method __ J_-_<_t-_,_P~"~.,,,.~~-~~~--------Sample lnterval __ c...J~"'~/~r ___ _
Appearance ______________ _ ,a_ ~ (f'ymp, b:.11.r, •It)
Field Analysis By: ____________ _ Remarks rJO,ccl v..}el( -V<»->d> f-,, t,v,, k, 5, , ,,Z 17
(pumplllQ tim•. u .fl'.ip_ •JC-)
LABORATORY ANALYSES
BOD 310 ma/I Diss. Solids 70300 mnn Ao -Silver 46566 unll
COD High 340 mg/I Flouride 951 mnn Al -Aluminum 46557 uatl
COD Low 335 moil Hardne<s· To1•1 900 m!,'l As -Arsenic 46551 unil
Colilorm: MF Fecal 31616 1100ml Hardness fnon-carbl 902 =' Ba -Barium 46558 unn
Colilorm: MF Total 31504 1100ml Phenols 32730 unn Ca -Calcium 46552 matl
TOG 680 mnl Snecific Cnnn. 95 uMhos/cm2 Cd -Cadmium 46559 un1I
Turbidity 76 NTU Sullate 945 m"" Cr -Chromium 46560 ua/1
Residue., Suspended 530 mg/I Sullide 745 ma/I Cu -Coooer 46562 ug/1
Fe -·Iron 46563 unn
V Ho -Mercurv 71900 :J. %'.'.> un/1
pH 403 units K -Potassium 46555 mQII
Alkalinity to pH 4.5 410 mg/I Ma -Maanesium 46554 m[j/1
Alkalinity to pH 8.3 415 mg/I Mn -Mannanese 46565 uatl
-
Carbonate 445 mg/I NH as N 610 mnn Na -Sodium 46556 mQII
Bicarbonate 440 moil TKN °• N <o< mn< Ni -Nickel unn
Carbon dioxide 405 m()l1 .,/ NO +NO as N 630 is', '.2 mn1I Pb -Lead 46564 unn
Chloride 940 mg/I P: Total a ... -----1\ 11 I \nn/1 Se -Selenium unA
Chromium: Hex 1032 U(l/1 r\r \rl , ... ,_~J Zn -Zinc 46567 un/1
Color: True 80 Pt-Co --. ~~r-.1,
Cyanide 720 mg/I ~rn '-i:. "'
Orqanochlorine Pesticides
Organophosphorus Pesticides
Nitroaen Pesticides
Acid Herbicides
r· -·
Semivolatile Organicd;:2 '., -:-:~
:r,,, c,~
-:-:u (•~~a~
V Volatile Organics (VC>l\'bottle) :,c:
:_..r-.-1 -,--1
TPH -Gasoline Range: ~.:;:;:;,;
TPH -BTEX Gasoline_ijange, ;:c: .. •·'-':::u -~.
--J r •1 '.
,
\ I
\/ .
Lab Comments: -----------,,.}ifl.01+LL"'tit>++IOBN1+C.1+0ll1Pt<l,..RO,.,,I__._B=RAcu
N
.
,
_
t
_
t
___________________ _
GW-54 REV. For Dissolved Analysis -submit tillered sample and write NOIS" in block.
!f-3 EHNR/DEM LABORATORY
VOLATILE ANALYTICAL REPORT
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE: WATER ANALYSIS RESULTS
TQL DETECTED
_______________________ ug/L __ ug/L_ CAS# VOA TARGET COMPOUND
75-35-4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-66-3
74-970 5
71-55-6
563-58-6
56-23c5
107-06-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-l
106-93-4
108-90-7
630-20-6
75-25-2
79-34-5
TQL-
T-
E-
U-
N-
D-
M-
COMMENTS,
1,1-Dichloroethene
Methylene Chloride
trans-1,2-Dichloroethene
1,1-Dichloroethane
2,2-Dichloropropane
cis-1,2-Dichloroethene
Chloroform
Bromochloromethane
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
Dibromomethane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Tetrachloroethene
1,3-Dichloropropane
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Bromoform
1,1,2,2-Tetrachloroethane
0.75
0.25
0.75
0.25
0.25
0.25
0.25
0.75
0.25
0.25
0.75
0.25
0.25
0.25
0.25
l
0.25
0.25
0.25
0.25
0.25
0.75
l
0.25
0.25
0.5
0.75
Target Quantitation Limit-Subject to
change due to instrument sensitivity
Tentatively Identified, not confirmed
Estimated Value
Samples analyzed for this compound but
not detected
Sample not analyzed for this compound
Detected below quantitation limit
GC/MS Analysis performed
0.59
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
CAS#
96-18-4
108-86-1
95-49-8
106-43-4
541-73-1
106-46-7
95-50-1
96-12-8
120-82-1
87-68-3
87-61-6
1634-04-4
71-43-2
108-88-3
100-41-4
108-38-3
95-47-6.
100-42-5
98-82-8
103-65-1
108-67-8
98-06-6
95-63-6
135-98-8
99-87-6
104-51-8
91-20-3
VOA TARGET COMPOUND
1,2,3-Trichloropropane
Bromobenzene
2-Chlorotoluene
4-Chlorotoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
l,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
Hexachlorobutadiene
1,2,3-Trichlorobenzene
Methyl-tert-butyl ether
Benzene
Toluene
Ethyl benzene
m,p-Xylenes
a-Xylene
Styrene
Isopropylbenzene
n-Propylbenzene
1,3,5-Trimethylbenzene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
p-isopropyltoluene
n-Butylbenzene
Naphthalene
Other purgeables detected
(up to 10 highest peaks)
NO VOLATILE ORGANIC COMPOUNDS DETECTED
BY GC/PID.
LAB NO. 4G332
SUPERVISOR~..
DATE u-,..•
ENTERED BY .
CHECKED BY
TQL
ug/L
0.25
l
0.25
0.25
0.25
0.25
0.25
l
0.25
0.25
0.75
5
l
l
l
2
l
l
l
l
l
l
l
l
l
l
l
DETECTED
ug/L
u
u
u
u
u
0.53
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Detected
ug/L
-
North Carolina
GROUNDWATER FIELD/LAB FORM /\H·ll I ri1 OF r.1 ISTfH'.,1·i V' Department of Environment, Health, and Natural Reoourco,
'.i_.,. !ri. !\ ' . vi. n \lJ'fi...DIVISION OF ENVIRONMENTAL MANAGEMENT-GROUNDWATER SECTION
County :1jrc;/.e /I
Quad No l'7o-o/ Serial No.______ SAMPLE PRIORITY el.,
Lat.------Long.--------:-]ROUTINE ['gJEMERGENCY
· -OcHAIN OF cusToov .
Report To: ARO, FRO,~?RRO, WaRO, WiRO, 0 Other: -----::c-:-----,--,,.--=--,------
Dala Entry By: _ _,@._,_,_, ___ Ck:~~----
WSRO, Kinston FO, Fed. Trust, Central Off., Other: ________ _ Dale Reported: ___:./~,,;;;2~0/2;7'1/t..:,===='"'J----
Shipped by: Bus Court , Hand Del., Other_· __________ _
I / Purpose:
Collector(s): -4-J-'-l-b"--'-"'"---Date 3 02 o/ '-I Time / 0: '(0 Baseline, Complaint, Compliance( LUST, Pesticide Study, Feder
-
I -m~,"!l. ',-..
EIELPANALYSES Owner ::E,e3, . .,o n11,/ fn,"c.,,t-) r:i.,1sv,,,urf,rw1 l;su laO/)
;, fr{;)'o/
pH'°° _ _,,b'-·-S,__Spec.Cond.9-4 ___ at25°C Locationorsite ':R:\. 1•1 Y3c,A" 35-5 F , >k1 te,uil.e
Temp.10
°c Odor Descriptionolsamplingpoint "'lP: te-P? c.i + c.ve 1(
Appearance
Sampling Melhod --:TcJ 1au=o 1
I. r°WU'T1',G,.,&;,.e1c)
Field Analysis By: Remarks D,=,, ,-; < w .. 4-s, 'if',e'i~
LABORATORY ANALYSES
,...,..,.,-_,.,.,,.., .• ,.,
Sample lnterval~'~·~t2=-~~~o~'--
BOD. 310 mgll Diss. Solids 70300 mn/1 AQ -Silver 46566 unll Oganochlorine Pesticides
COD High J.<10 mg/1 Flouride 951 mnll Al -Aluminum 46557 unil Organophosphorus Pesticides
COD Low 335 mQ/1 Hardne~~·Tntal900 mg,1 As• Arsenic 46551 unn Nilroqen Pesticides
Coliform: MF Fecal 31616 1100ml Hardness tnon·corbl 902 =" )( Ba -Barium 46558 /'"-0 unil
Coliform: MF Total 31504 1100ml Ph•~ls "730 un11 Ca -Calcium 46552 mnl\ Acid Herbicides
TOG 680 mnl ~ Specific Cond, 95 uMhos/cm2 X Cd -Cadmium 46559 < ·, . D unn
Turbidity 76 NTU Sulfate 945 =" Cr • Chromium 46560 ua/1 Semivolatile Organics
Residue., Suspended 530 mg/1 Sulfide 745 mn/1 ✓ Cu -Conner 46562 14' un/1
>< Fe • Iron 46563 <:5r, un/1
'--·' ' .-, i ~·1
y Hg• Mercurv 71900 0,7',0 ua/1 X Volatile Organics (VOl\"bottle)· _
pH403 unit, K -Potassium 46555 mg(
::-,] ~',-~ f;·1
Alkalinity to pH 4.5 410 mg/1
Mn . Maanesium 46554 mn1 TPH -Gasoline Range°'.'. '"-~~(,-;
Alkalinity to pH 8.3 . 415 mg/1
✓ Mn -Manoanese 46565 . ? .;i_ un/1 TPH -BTEX Gasoline-Bang~:,>:
Carbonate 445 mg/1 NH aa N 610 ma/I .x Na . Sodium 46556-'>, .o;L. ~ "'."""' :.·:~J
Bicarbonate 440 mn/1 7 "tllM .... N r-,c: =" y Ni -Nickel «"tO ugil
,. ;;~~ i: 1 -"•
Carbon dioxide 405 mQ/1 x· NO +NO as N 630 L/-' '-+ =" x Pb -Lead 46564 ',L 5 un/1
-.. .J i-=-1 :.;'.: ::li :·----
Chloride 940 mg/1 P: T o1al as P £6"'•--~ r H " Se • Selenium un/1 \ I ·-(.'1 -
Chromium: Hex 1032 ug/1 'it1_\,i •Hr ) I >< Zn -Zinc 46567 /90 un/1 \ I .. s·-.:
Color: True 80 Pt-Co
V
Cyanide 720 mg/1
n1~·i \ L ,~ Ii r,·.
Lab Comments: ----------->\l'f-lQ+![L++Yl+fi.lOf;l'~µj Crt10-aNT>l-lBMUluBmR,..AN..uf'u...t ___________________
_
GW-54 REV .. For Dissolved Analysis• submil filtered sampfe and write ·ms· in blClf"k.
LAB NO.
BHNR/DEK LIJlORATORY
VOLATILE ANALYTICAL REPORT
REPORTED BY
CHECKED BY
RBVIBWBD BY
SUPERVISOR~K. DATE .3 5c -'
ENTERED BY
CHECKED BY
SAMPLE TYPB: WATER
CASI VOA TARGET COMPOUND
75-35·4 1,1-Dichloroethene
75-09-2 Methylene Chloride
156-60·5 trans-1,2-Dichloroethene
75-34-3 1,1-Dichloroethane
590-20-7 2,2-Dichloropropane
156-59·4 cis-1,2-Dichloroethene
TQL
u
0.75
0.25
0.75
0.25
0.25
0.25
ANALYSIS RESULTS
CASI VOA TARGBT COMPOUND
u 96-18-4 1,2,3-Trichloropropane
u 108-86-1 Bromohenzene
u 95-49-8 2-Chlorotoluene
u 106-43-4 4-Chlorotoluene
u 541·73·1 1,3-Dichlorobenzene
u 106-46-7 1,4-Dichlorobenzene
67·66·3 Chloroform 0.25 0,29 T 95-50-1 1,2-Dichlorobenzene
74-97-5 Broaochloromethane 0.75 u 96-12-8 1,2-Dibromo-3-Chloropropane
71-55-6 1,1,l·Trichloroethane 0. 25 u 120-82-1 1,2,4-Trichlorobenzene
563-58-6 1,1-Dichloropropene 0. 25 u 87-68-3 Hexachlorobutadiene
56-23-5 carbon Tetrachloride 0.75 u 87-61·6 1,2,3-Trichlorobenzene
107-06-2 1,2-Dichloroethane 0.25 u 1634-04·4 Methyl-tert·butyl ether
79-01·6 Trichloroethene 0.25 u 71·43·2 Benzene
78-87·5 1,2-Dicbloropropane 0.25 u 108-88·3 Toluene
75-27-1 Bromodichloromethane 0.25 u 100-41-4 Ethyl benzene
71-95-3 Dibromoaethane 1 u 108-38-3 m,p•Xylenes
10061·01·5 cis-1,3-Dichloropropene 0.25 u 95-47-6 a-Xylene
10061-02·6 trans-1,3-Dichloropropene 0.25 u 100-42-5 Styrene
79·00·5 1,1,2-Trichloroethane 0.25 u 98-82-8 Jsopropylbenzene
127-18-4 Tetrachloroethene 0.25 u 103-65-1 n· Propylhenzene
142-28-9 1,3-Dichloropropane 0.25 u 108-67-8 1,3,5-Trimethylbenzene
124·48·1 Dibromochloroaethane 0.75 u 98-06-6 tert•Butylbenzene
106-93-4 1,2-Dibromoethane 1 u 95·63·6 1,2,4-Trimethylbenzene
108-90-7 Chlorobenzene 0.25 u 135-98·8 sec-Butylbenzene
630·20·6 1,1,1,2-Tetrachloroethane 0.25 u 99-87-6 p-isopropyltoluene
75-25-2 Bro1ofor1 0.5 u 104-51-8 n-Butylbenzene
79-34-5 1,1,2,2·Tetrachloroethane 0.75 u 91-20-3 Naphthalene
TQL· Target Quantitation Limit· subject to other purgeables detected
change due to instrument sensitivity (up to 10 highest peaks)
T-Tentatively Identified, not confiraed
E· Estiaated Value NO VOLATILE ORGANIC COMPOUNDS
U· samples analyzed for this compound but DETECTED BY GC PIO.
not detected
N· sample not analyzed for this compound
D-Detected below quantitation limit
K-GC/KS Analysis perforaed
COMMENTS:
0.25
1
0.25
0.25
0.25
0.25
0.25
1
0.25
0.25
0.75
5
1
1
1
2
1
1
1
1
1
I
1
1
1
1
1
Detected
ug/1
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
..
. ~
GROUNDWATER FIELD/LAB FORM,...,q i-[' H\l Gt
• -:t1·~\c_1;,·.
·-I){)'V North Carolina
f' ~ \ 'S \ \J \ . i Department of Environment, Health, and Natural Rnources
u;l,, °" ·-DIVISION OF ENVIRONMENTAL MANAGEMENT-GROUNDWATER SECTION
County_~;:t:«----r_,oe,£"'-"-e_ll ________ _
'7-
Lab Number 2l
Serial No. _____ _
Quad No Ll7n-7
Lat. 5:,0 (/;) I 5 '7 11
SAMPLE PRIORITY
Long. frn°5'1' 12 ''
Rec'd by: [)s From: Bus, ~Hand Del.,
r:71ROUTINE □EMERGENCY 0
Date Received )-1 fo-9 L:\ Time '2:2,.:,()
l:'.::J Other: -----,------,...,_.,.... ___ _
r.:.::::,, [ijcHAIN OF CUSTODY @' Ti5
Report To: ARO, FRO,'Ml:lk/, RAO, WaRO, WiRO,
Data Entry By: Ck:_,,;,;:___..~---
WSRO, Kinston FO, Fed. Trust, Central Off., Other:________
Date Reported:'--/'--'0¼-'-~....c.c6"'1'""~.....,,--------
Shipped by: Bus,@l, Hand Del., Other·____________ Purf>)so: . . c~~Cle,~'_1 __ 3~
Collector(s): I\ no /I If Date -:JI t:r/1 '( Time ~l~/:_o~,; ___ Basohne, Compla,nt, Compl,anco, LUST, Pest1c,ae-s1uoy.rodoral Trust, Other: ~/s~o_((_. ~,l~/02~· ~---
) ,m•o~I /1 /
Fl ELD ANALYSES Owner Afr. k&&-1 .fo ,,,P ( Tccy,"'1°+;; /TI lri {,.,,,,, ,,1,:,c = G,v.aec/
Localionorsite '.fu,k /'-/ ISav:3::,'7 s-1-u.foo,·II( ?~G?7
Description ol sampling point -.1-"-+''-'"--'-./--'w""'-<c..;lc.1 ____________________ _
Sampling Method ___ p,..,~,,.,,_,~.,.,,,._-~-~---------Sample lnterval_,.,~,,,_l(~----
v-I (Pl.W_T'41.6aii.r.f;,l
Remarks U~, r -Lr r.A.Jt,;c ~ .--I!? pl t.,(,' 1 r
pH'°" ____ Spec. Cond.94 ___ at 25° C
Temp.10
°c Odor. _____ _
Appearance ______________ _
Field Analysis By· ...'.ll s -" ~, r JI {pumJ)ll'lO 11'"41, ai' I~. el~;,
LA60BAIOB)'. ANAL)'.SES ()lo.oct' OV'CAlt.r ze. . / 11,,,-,, :I{ e,, __ ,, __ / e-.,. .H {o,
BOD. 310 mn/ Diss. Solids 70300 ~· Ag -Silver 46566 una Oraanochlorine Pesticides
COD High 3"0 mg,1 Flourido 951 mnlt Al -Aluminum 46557 . ua/1 Organophosphorus Pesticides
COD Low335 mall Hardness· Total 900 mn• As -Arsenic 46551 unA Nilrogen Pesticides ~:,
Colilorm: MF Focal 31616 1100ml Hardness Cnon-carb) 902 mn/1 Ba -Barium 46558 un/1 ~-_Q ~-!
Colilorm: MF Total 31504 1100ml Ph•nols "730 un• Ca -Calcium 46552 =II Acid Herbicides -~ : -, ?:J
TOG 680 mal1 S=cilic """" 95 uMhos/cm' Cd . Cadmium 46559 unit
-•.J ~:-~'c-)
-·-·
Turbidity 76 NTU Sullate 945 mn/1 Cr -Chromium 46560 unit Semivolatile Organics ,.,__., ::.:: :__.. ·-·-, --
Residue., Susperidod 530 mg,1 Sullido 745 mall Cu • Conoor 46562 ua/1
'•J :..-..] { ·:;
n
.x._ Fe -Iron 46563 < .. "J 0 ua/1
~;:.,-. s~:-~:-: .
y Hg -Mercury 71900 0, !i'x' ua/1 X Volatile Organics (VOA bo~I•) ;:;., :',
pH403 unit, K -Potassium 46555 ma/
.. ,.,. ,J :0 ·-•0
Alkalinity lo pH 4.5 410 mg,1 Mn -Maanesium 4655-4 mQ/1 TPH -Gasoline Range . .J I ~-1
Alkalinity to pH 8.3 415 mg,1 'x Mn -Mannaneso 46565 '79' unit TPH -BTEX Gasoline Range
Carbonate 445 mg,1 NH. as N 610 mnlt Na -Sodium 46556 mQII
Bicarbonate 440 mn/1 ITKN •• N ~,. =" Ni -Nickel unA
Carbon dioxide 405 mn/1 )( NO +NO asN 630 /I, 5 !!.'9'!... Pb . Lead 465G4 unn
Chloride 940 mg,1 P: Total as P 665 mnn Se -Selenium unit /
Chromium: Hex 1032 ug/1 ✓ Zn -Zinc 46567 7 _"! ua/1 I
Color: True eo Pt-Co
V
Cyanide 720 mgtl
Lab Comments: ________________________________________________
_
_
_
_
_

_
GW-54 REV. For Dissolved Analysis -submil tillered sample and write ~DIS" in blcv-k.
EHNR/DEM LABORATORY
VOLATILE ANALYTICAL REPORT
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE: WATER ANALYSIS RESULTS
CAS# VOA TARGET COMPOUND TQL DETECTED
ug/L _ug/L_ -------------------------
75-35-4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
563-58-6
56-230 5
107-06-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79034-5
TQL-
T-
E-
u-
1,1-Dichloroethene
· Methylene Chloride
trans-1,2-Dichloroethene
1,1-Dichloroethane
2,2-Dichloropropane
cis-1,2-Dichloroethene
Chloroform
Bromochloromethane
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
Dibromomethane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Tetrachloroethene
1,3-Dichloropropane
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Bromoform
1,1,2,2-Tetrachloroethane
0.75
0.25
0.75
0.25
0.25
0. 25
0.25
0.75
·0.25
0.25
0.75
0.25
0.25
0.25
0.25
1
0.25
0.25
0.25
0.25
0.25
0.75
1
0.25
0.25
0.5
0.75
Target Quantitation Limit-Subject to
change due to instrument sensitivity
Tentatively Identified, not confirmed
Estimated Value
Samples analyzed for this compound but
not detected
N-Sample not analyzed for this compound
D-Detected below quantitation limit
M-GC/MS Analysis performed
COMMENTS:
u
u
u
0.71
u
1.4
D
u.
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
CAS# VOA TARGET COMPOUND
96-18-4 1,2,3-Trichloropropane
108-86-1 Bromobenzene
95-49-8 2-Chlorotoluene
106-43-4 4-Chlorotoluene
541-73-1 1,3-Dichlorobenzene
106-46-7 1,4-Dichlorobenzene
95-50-1 1,2-Dichlorobenzene
96-12-8 1,2-Dibromo-3-Chloropropane
120-82-1 1,2,4-Trichlorobenzene
87-68-3 Hexachlorobutadiene
87-61-6 1,2,3-Trichlorobenzene
1634-04-4 Methyl-tert-butyl ether
71-43-2 Benzene
108-88-3 Toltiene
100-41-4 Ethyl benzene
108-38-3 m,p-Xylenes
95-47-6 o-Xylen~
100-42-5 Styrene
98-82-8 Isopropylbenzene
103-65-1 n-Propylbenzene
108-67-8 1,3,5-Trimethylbenzene
98-06-6 tert-Butylbenzene
95-63-6 1,2,4-Trimethylbenzene
135-98-8 sec-Butylbenzene
99-87-6 p-isopropyltoluene
104-51-8 n-Butylbenzene
91-20-3 Naphthalene
Other purgeables detected
(up to 10 highest peaks)
NO VOLATILE ORGANIC COMPOUNDS DETECTED
BY GC/PID.
LAB NO. 4G331
SUPERVISOR "Jk''ll
DATE . ~' !f_
ENTERED BY ~i
CHECKED BY/<
TQL
ug/L
0.25
1
0.25
0.25
0.25
0.25
0.25
1
0.25
0.25
0.75
5
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
DETECTED
ug/L
u
u
u
u
u
D
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Detected
ug/L
-
State of North Carolina
Department of Environment,
Health and Natural Resources
Mooresville Regional Office
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
Vivian H. Burke, Regional Manager
NA
DEHNR
DIVISION OF ENVIRONMENTAL MANAGEMENi?
February 15,
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
Mary L. Sigmon
A.A.A. Enterprises, Incorporated
Route 14, Box 350
t10LLUT/ON CONTROL BRA(~C:
Statesville, North Carolina 28677
Subject: Request for Modification
Dear Ms. Sigmon:
to Lagoon Closure Schedule
(A.A.A. Enterprises)
Groundwater Incident W 3422
Iredell County, N.C.
I have reviewed Steve Burrows' response, on your behalf, to
the Division's December 21, 1993 Notice of Regulatory
Requirement. I also spoke with Mr. Burrows on January 10, 1994,
concerning your request to use lagoon W 1 as a liquid storage
pond for the proposed composting project. Based on my
conversation with Mr. Burrows and the information presented in
his letter, the Division will allow lagoon 1 to remain open until
July 1, 1994.
Lagoon 8 should have already been closed and documentation
to that effect should have been submitted by February 1, 1994 to
this office. A review of the file for this site, indicates that
the documentation has not been received. Failure to submit the
required documentation within seven days of receipt of this
letter may result in a recommendation for enforcement beginning
from February 1, 1994.
If you have any questions, please contact me at (704) 663-
1699, ext. 235.
s~ely,
Chris'D~
Hydrogeologist
cc: Groundwater Section -Raleigh
Steven Burrows -Shield Environmental Associates
CMD/sc
919 North Main Street, Mooresville, North Carolina 28115 Telephone [phone] FAX [phone] ,
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post•consumer paper
' . State of North Carolina
Department of Environment,
Health and Natural Resources
Mooresville Regional Office
Jomes B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
Vivian H. Burke, Regional Manager
DIVISION OF ENVIRONMENTAL MANAGEMENT
December 21, 1993
CERTIFIED MAIL
RETURN RECEIPT REQUESTED ~AN 2 0 1994
Mary L. Sigmon
A.A.A. Enterprises, Incorporated
Route 14, Box 350 POLLUTION CONTROLBRAN_QJ! ~
Statesville, North Carolina 28677
Subject: Notice of Regulatory Requirement ')
15A NCAC 2L Classifications
and water Quality Standards
Applicable to the Groundwaters
·,_,,?J ., ,..,
;n r-·J C?:i·,1 (_, __ _
: :-.-:: ~2 ?:~ I~~
1·1·1 .. :
., ~; J
:.,..) ~ I)
Dear Ms. Sigmon:
Sigmon Septic Tank Service
(A.A.A. Enterprises)
Groundwater Incident W 3422
Iredell County, N.C.
...J r"1
C)
Staff of the Mooresville Regional Office Groundwater section
has reviewed the sampling results and proposed closure plans for
the subject site. The results indicate that numerous compounds
are present in lagoon sludges at concentrations exceeding the
Division's soil and groundwater action levels.
15A NCAC 2L .0106(f)(3) and (4) require that primary and
secondary pollution sources be removed, treated, or controlled
prior to or concurrent with assessment activities. In order to
comply with these rules, the lagoons must be properly closed and
contaminated sludges and soils must be treated, contained or
disposed of in accordance with rules and procedures established
by the Division.
On-site containment and treatment of the contaminated sludge
is acceptable provided that you first obtain a non-discharge
permit for soil remediation. A permit application is enclosed
for your use. Lagoons 1 and 8 may be closed by liming and
backfilling with clean soil.
919 North Main Street, Mooresville, North Carolina 28115 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post-consumer paper
A.A.A. Enterprises, Inc.
December 21, 1993
Page Two
A review of boring logs for the Division's monitor wells
prepared by the regional hydrogeologist indicate that sand and
silt are the predominant soil grain sizes at depths below nine
feet. The Groundwater Staff revised the site sensitivity
evaluation form accordingly and the action levels for 5030 TPH
and 3550 TPH are now 40 parts per million (ppm) and 160 ppm,
respectively, provided that you can demonstrate a ten-foot buffer
zone between the seasonal high water table and soils containing
5030 TPH and 3550 TPH at concentration of 10 ppm and 40 ppm,
respectively. Please be aware that data available to date are
not sufficient to demonstrate this.
Lagoons 2 through 7 have TPH levels above the SSE action
levels. Several volatile organic compounds are also present in
concentrations well above North Carolina's groundwater standards.
Low levels of many of these compounds have been detected in the
groundwater at the site. Therefore, contaminated sludge and soil
must be removed and treated from these lagoons.
Confirmatory samples must be collected from the soils
remaining in place in these lagoons. The samples should be
analyzed for TPH using sample preparation methods 5030 and 3550
with the California GC Method and for volatile organic compounds
using Method 8240. ·
In addition, due to the detection of leachable cadmium and
lead in sludge samples collected from the lagoons, a background
soil sample must be collected and analyzed for TCLP metals. If
the concentrations in the sludge are significantly higher than
these in the background sample, confirmatory soil samples must
also be analyzed for TCLP metals. ·
I have attached an implementation schedule for closure of
the lagoons. If you have any comments or concerns about the
schedule, please contact Chris DeRoller by January 15, 1994.
Upon closure of the lagoons, Groun.dwater Section Staff will meet
with you to discuss groundwater monitoring and remediation
options for the site. Please be advised that a thorough job of
sludge and soil cleanup initially should significantly reduce
future monitoring and remediation costs.
Failure to respond within the time specified and to
voluntarily achieve compliance may result in a recommendation for
enforcement, as described in the Notice of Violation issued to
you on July 13, 1993.
A.A.A. Enterprises, Inc.
December 21, 1993
Page Three
If you have any questions, please call Chris DeRoller or me
at [phone].
Sincerely,
D.t?~ Jr~~
Brenda J. Smith, P.G.
Regional Supervisor
Attachment: Schedule of Implementation
Soil Permit Application
cc: Groundwater Section -Raleigh
Steve Burrows -Shield Environmental Associates, Inc.
(with attachments)
CMD/sc
State of North Carolina
Department of Environment,
Health and Natural Resources
Mooresville Regional Office
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
Vivian Burke, Regional Manager
.NA
DEHNR.
DIVISION OF ENVIRONMENTAL MANAGEMENT
July 13, 1993
RECl=I\IFO
JUL ' 9 \993
CERTIFIED MAIL o BRAMCH RETURN RECEIPT REQUESTED POLLU110N CONTR L ,~
Mr. Barry Sigmon
A.A.A. Enterprises, Incorporated
Route 14, Box 350
Statesville, North Carolina 28677
RE: Notice of Violation
Dear Mr. Sigmon:
15A NCAC 2L Classifications and
Water Quality Standards Applicable
to the Groundwaters
Sigmon Septic Tank Service (AAA Enterprises)
Groundwater Incident W 3422
Iredell County, N.C.
On August 9, 1990 you were issued a Notice of Violation
(NOV) from the Division of Environmental Management (DEM) for
violation of the North Carolina Groundwater Standards (15A NCAC
2L .0202). In the NOV you were required to determine the
vertical and horizontal extent of soil and groundwater
contamination and to submit a site assessment report within 60
days of receipt of the NOV. The NOV was held in abeyance pending
a review by the Hazardous Waste Section of the Division of
Environmental Management. In April of 1993, the Hazardous Waste
Section concluded that the site did not fall under its
jurisdiction.
On May 5, 1993 staff from the Mooresville Regional Office
Groundwater Section resampled two of the monitor wells at the
subject site and found that groundwater standards violations
still exist at the site. Specific violations are as follows:
919 North Main Street, Mooresville, North Carolina 28115 Telephone [phone] FAX 704-663·6040
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post-consumer paper
' AAA Enterprises, Inc.
July 13, 1993
Page Two
Constituent
dissolved solids
nitrate
mercury
lead
2-chlorotoluene
1,4-dichlorobenzene
benzene
1,3,5-trimethylbenzene
n-butylbenzene
naphthalene
Concentration*
650,000
54,000
29
75
2
6.1
2.3
1
1 . 6
1 . 3
2L Standard
500,000
10,000
1 . 1
50
ND
*
1 • 8
1 . 0
ND
ND
ND
* Concentration in micrograms per liter (parts per billion).
ND Not permitted in detectable concentrations.
The Groundwater Section staff also sampled two downgradient
water supply wells in February of 1993 and found that both wells
contained nitrate levels above the groundwater standards.
You are responsible for causing the continuing violation of
the underground water quality standards because you have stored
and/or disposed of septage waste in unlined lagoons. According
to 15A NCAC 2L .0106 (c)(1), you are required to assess the
cause, significance and extent of the violation, submit a plan
and schedule for eliminating the source and for restoration of
the groundwater; and implement an approved plan in accordance
with a schedule established by the Director. In establishing a
schedule, the Director shall consider any reasonable schedule
proposed by the person submitting the plan.
To achieve compliance with the above-cited laws or rules,
you are required to submit within sixty (60) days from receipt of
this letter a site assessment report in accordance with the
enclosed guidelines. This data will then be used to submit a
corrective action plan which will be due within sixty (60) days
after the site assessment report is submitted and approved by
this Office.
In addition, 15A NCAC 2L .0106(b) states that any person
conducting or controlling an activity which results in the
discharge of a waste, hazardous substance or oil to the
groundwater, or in proximity thereto, shall take immediate action
to terminate and control the discharge, mitigate any hazards
resulting from exposure to the pollutants and notify the
Department of the discharge. To comply with this section of the
rules, you must provide an alternate drinking water supply for
the residents who use the wells at Route 14, Box 356 and Box 357
(the last two wells on the dirt road behind your facility) within
seven days of receipt of this letter.
AAA Enterprises, Inc.
July 13, 1993.
Page Three
You should be aware, however, that the above violation of
15A NCAC 2L may subject you to a civil penalty assessment under
the authority of G.S. 143-215.6a of up to $10,000 per rule
violation. each day that the violation continues may be
considered a separate violation. Failure to respond within the
time specified and to voluntarily achieve compliance may result
in a recommendation for enforcement, the issuance of a Special
Order against you under the authority of G.S. 143-215.2, or a
request to the Attorney General to institute an action for
injunctive relief.
Your response and/or questions should be directed to Chris
DeRoller of the Mooresville Regional Office at [phone],
ext. 235.
Sincerely,
~1.~-th Brenda J. Smith, P.G.
Regional Supervisor
cc: Groundwater Section, Raleigh
Laurie Martin, Hazardous Waste Section
Julian Foscue, Solid Waste Section
Rhonda Morgan, Well user
Bill Munford, Well user
Enclosures: Site Assessment Guidelines
Sample Results
VUU\l I l
LONG. S-o
LAB NUMBER 8 ' ) t;:, 'i u I\ Department of Environment, Health, and Natural Resources c: // ) c o -r ,-. . . . DATE RECEIVED, )Q ·J Time()~"'::)·',
5
s Os ,, D1v1s1011 of Env1ronmenlal Management . TY; .,.-2------:------..
.. _Gr911f\.9raJ~r,.f10Jr~~Nl.f PH~. --' , .. -~•c d by . rrom □u~•
Roporl lo: ARO, FRO, ~Cl) RAO, WaRO, WiRO, ~HMJN ut cu~1uvYr','@'l',!'1F:id1hor
SAMPLE PRIORITY l',1 6 \9S:i DATA ENTRY BY: 71( CK· bJ..-7 WSAO, Kinslon r-o 0th or _________ _ = D J &/30/0 ~ ROUllNr (t,HflC!-/lCY OAIS,,1Hf'Oll1£D .. ________ . ____ _ ~)hippod !Jy: Ou!.,cc·~·urio;.~ Otllur _______ _ ,,;, ,' h'Lll t.t.{f\\~(.\~
COLLE CTORf SJ -Q,2;, II .if h1 h //:ci DA TE
FIELD ANALYSES
PH-4 00 7,0 Spee, Cond. 94 55i) a I .2-5"e--C
Ownor
TIME /v.'/0 /1! YJ/PURPOSE: BAS~~~~:· CO~PL0~i~rr, COfAPLIANCE, LUST, OTHER Pa I I r,.., '---'
(clrclu on•)
JtJ1,'.11 ... 1 ,,--,. 1 .f.,-,-,j),,('~, c5-
I
~-:•,-/)r,c
I
'S ,,e-[(,;;:cr .l
· .......
(J-<?r ·3 Y:t?-.: ---~---------··--~~ location or sJ 10 s. ,-::. i I -:, __ , ·~ -, /4..-(<; .,..., '·-+-o ,.--I± J
Te mp. 1 0 --~-· 0c Odor -~O~Ci-c<l;,Y~'~•Li~c__,G"i""a,1y De sc r J p Ii on ol sarnpl i no :JOJ n I
Appearance ();,t.<y l!;.1c&,ic/ Tas10 __ ,,,._,._-L/..cf"!_·c..• __ _ _.. I . . Sampl i nQ Me th od . __ Sa rnpl a l nt or v a I -~~?,_:~-c._·-~.3"-'o""-------
FI e Id Ana I y s i s By: ~(,u,="~' .. luk_e~( _____ _
(r,ump, bollor, e1cJ
A em J f k s ,1~·.u=--~<~---~'i<-"~, _,"/'--+---~-~s'--cc~~, ~n~. _/~,~·~, -"--"---1="-'0-''-''-''-'''-'-C-',t _ _,,,_-~--~··-''~'-''--'f-'c"--·~'~·,~-,..c,~•>c-.,, Cc...:l-''~•~2~'',-----',L-=--• ·c..· -'-/~,~-~~L~---· '(nurnplno !lrne, air 1om1p, ale-:-)
,~Lf;..:L( .... : .. f:!....c__l:::...!...1____F(..~:c-_'.'_£...:~· __ .,,, I AIJOflAIOIIY ANAi y:;1>;
-B()UbJIO mo/I V' Dh,. Solid• IOJOO +.;io mg/J Ag· Sll~•I 1 0 T 1 uo/1
coo t1Jon J" molt Fluoride IIS I rno/1 Al • Al1m1l11um 1 IO 5 u g/1 Org1nopho1p/'.oru1 r,11lold11
COD Lo .. '" mg/I H11dn,u:Tol1J 000 mg/J )<. o, -a.,1um ·1001 110 "°" X Co1Jrotm;l.4F r, c,J J161B..c/ao 1100ml H.,dn111 (non•cub) 002 mg/I c, • Calcium ". mg/I
Colllorm:l.4F lohl J 1 so 4 1100ml Ptuno/1 J21JO "°" Cd • Cad<'llum 1027 UQ/1
TOC 6no mo/I Sp,clllc Cond. " uMho1/cm 1 Ctuomlum:To11t 1 OJ~ ug/t
Turbldll1 " NTU Sulr11, 9 ◄S mo/I Cu -Copp11 10◄ 2 ug II
Sulllch '" mo/I Fo • Iron IO ◄~ uo/1
. ')( Hg · Lle,cu,y 71',IOO < (-i, :'1-uo/1 ~.,.-Purgt1bJ1 Oroanlct {YOA borll•J
'" <OJ uni lo K -Po11,olum QJ1 moll
Alk•llnlly lo DH ◄. ::0 .,. mo/I "' 1.1,or••••"rn Q21 m<>'•
AlkttlnlLr " OH ,., "' mg/I "". l.l1ni.,•n••• 1056 uo/1
Carbontl• .. ' mg/I "' Sodium '" mo/I
Blcarborut, ◄ .• 0 mo/I y Nt1J .. N 6 10 0, 7;)_ mg/I NL NI ck• J 1061 UQ/1 ·•··· "' ,o.ro Aruntc:1011! 1002 "°" !KN .. N 625 mo/I y' Ob · L • • d 10~ I h.~ ug/1
C11bon a"!o1ld• ,o, mo/I )< NOJ: • NOJ 11 N 6JO 7,3 mg/I s, -s,1u1lum 11 ◄

7

UQ /l
Chlorld, 'i~O mQII P:Toul u P 665 mg/I '" -Z Inc 1091 UQ /l
Chromlvm:H• • 10)1 uo /I
Color:lr'-"" eo Pt·Co
-Cy,nld• "" mg/I
Lab Comments:
c' r
I
GW-5-4 REY. 9/90 for Dlssolvod Analysis -submli Jlttorod sample and wrile ·01.0 • 11 block
While Copy -Groundwalar Conlral 0111ce Yellow Copy -f · · · mal 0/f\cQ flnK Copy -Cenlral flle1 Goldenrod C,,nv , I •h
JHNR/DEK LABORATORY
VOLATILE ANALYTICAL REPORT
LAB 110, JG 701
~ 1! SUPERVISOR. REPORTED BY
CHECKED BY tlif DATE S,1,;ig '13
REVIEWED BY ENTERED BY ( S'S(i C-·
CHECKED BY ,C
SAMPLE TYPE: WATER AIIALYSIS RESULTS
CASI VOA TARGET COMPOUND DETECTED CASI VOA TARGET COMPOUND TQL nmmD
u 1 u 1 uo 1
75-35-4 1,1-Dichloroethene 0, 75 u 96-18-4 1, 2, 3-Trichloropropane 0,25 u
75-09-2 Methylene Chloride 0 , 2 5 u 108-86-1 Broiobenzene 1 u
156-60-5 trans-1,2-Dichloroethene 0, 75 u 95-49-8 2-Chlorotoluene 0, 2 5 u
75-34·3 1,1-Dichloroethane 0,25 0, 41 T 106-43-4 4-Chlorotoluene 0.25 u
590-20-7 2,2-Dichloropropane 0,25 u 541-7J-l 1,3-Dichlorobenzene 0. 2 5
156-59-4 cis-1,2-Dichloroethene 0,25 0.51 T 106-46-7 1,4-Dichlorobenzene 1. 2 5 6, 1
67-66·3 Chlorofor~ 0,25 u 95-50-1 1,2-Dichlorobenzene 0,25 G.13 T
74-97-5 Bro1ochloro1ethane 0,75 u 96-12-8 1,2-Dibro10-J-Chloropropane 1 u
71-55-6 1, 1, !-Trichloroethane 0,25 u 120-82-1 1, 2, Hrichlorobenzene 0, 2 5 u
56i-58-6 1,1-Dichloropropene 0,25 u 87-68-3 Hexachlorobutadiene 0, 15 u
56-23-5 Carbon Tetrachloride 0,75 u 37-61-6 1,2,3-Trichlorobenzene 0 , 7 5 u
107-06-2 1,2-Dichloroethane 0,25 u 1634-04-4 Hethyl-tert-butyl ether u
79-01-6 Trichloroethene 0, 2 5 u 71-43-2 Benzene u
78-87-5 1,2-Dichloropropane 0, 2 5 u 108-88-3 Toluene 1 u
75-27-4 Bro1odichloro1ethane 0,25 u 100-41-4 Ethyl benzene 1 .. ' ' 74-95-J Dibromethane u 108-38-J m,p-Xylcncs 2 )
10061-01-5 • cis-1,J-Dichloropropene 0, 2 5 u 95-47-6 o-Xylene 1 u
10061-02·6 trans-1,J-Dichloropropene D.25 u 100-42-5 Styrene u
79-00-5 1,1,1-Trichloroethane 0, 2 5 u 98-82-3 Isopropylbenzene u
127-18-4 Tetrachloroethene 0,25 u lOJ-65-i n-Propylbenzene u
142-28-9 1,3-Dichloropropane 0.25 u 108-67-8 1,3,5-Triiethylbenzene u
124-48-1 Dibro,ochloromethane 0,75 u 98-06-6 tert~outylben2ene u
106-93-4 1,2-Dibroioethane 1 u 95-63-6 1,2,4-Triaethylbenzene D f
108-90-7 Chlorobenzene 0,25 0, S 1 T 131-98-8 sec-But1lben1ene u 630-20-6 1,1,1,2-Tetrachloroethane 0, 2 5 u 99-87-6 p-isopropyltoluene u
75-25-2 Broioforn 0, 5 u 104-51-8 n-Butylbenzene ' , . , , 0 i
19-34-5 1,1,1,2-Tetrachloroethane 0, 7 5 u 91-20-3 llaphthalene
TQL-Target Quantitation Limit-subject to Other purgeables detected ,etccted
change due to instrument sensitivity (up to 10 highest peaks) ug/l
T· Tentatively Identified, not confirmed
E· EstiJated Value
u-sa1ples analyzed for this co1pound but
not detected
II· Sample not analyzed for this co1pound
D-Detected below quantitation limit
K· GC/KS ~nalysis performed
COHHENTS:
SERI Al NO.
LONG . ;-y,,0 ,.-.f
y, I r LAB NUMBER 8 ~-(, ·:3 {{\.(0\ Department of Environment, Health, and Natural Resources "--, o., ic-:-
DATE RECEIVED Tim.• _ _'_):_ 'j ) Division of Environmental Man2Jement ~
Groundwater Field/Lab Forrn t)t"il""'t:Af~}t°f'~\JJ") Frnm: suE_-,0
neport lo: Ano. Fno(!~D\ RAO, WaRO, WiAO, C~JM; @~oti~ldSTOOY G; 'orhar
cf_,.,~~9,.;1TRY □Y· c;.IJ CK: J):__~ WSnO, Kinslon FO Olhor
Shipped by: □us.~;~)r, Olhor _______ _ [SJ nOUTINE □ EMERGENCY DATE REPOJJHiD· , <,)<,O/lJ POLLu 1 .. : ', CUN i KUL t'.Kn1~Ct1 --~~'-""c__ ___ _
COLLE C TO n ( S ) : n, /1,r:fL. /;1_),/((.,£,1
' DATE TIME PURPOSE: BASELINE, COMPLAltJT, COMPLIANCE, LUST, OTHER ~/_'4_-•_I_I_:?_~_,_,_'-_·
{circle on-.)
FIELD ANALYSES gco 0 wnor ·~(~ (:,,is ( 5, Y1"1Y! _( ,, _<;-_,Jl'rP
7o k"1' I
Spec. Cond. 94 ., .. ~t locarion or sl lo S.p { I , .. ,/ C, , I 4:,r
Odor _c,,I _____ _ Description al sarnplino polnl o-f-
Appearance ·K,cJ(rc~lJ/J Tasia --"-~"-'-V,.'-4 __ _ · ,,,,,t,,, ,:;:l.'. SamplinQMathod Sk_c; f~.k-L;~..... __ sample fnlorval _--?o -uo
(pump, boilor, otc
Field Analysis By: SvJ'!-,/(-?( Romarks 5-•~1·(. ;3o ;, S Y '/;:; -:=.,-,. //,·. 1 L,.,,'(,.< f ,;:',,.-.,, 1---<:" s1~-,.,_,.1;,_1 ,{_,_1,-·../. ......-,; £.J
I AIJ0flATOl1Y ANALYS[S -
fi (pumplo-o tlmo. ·air 10mp; MIC.)
-,"-'•L'LC~(JC;_,.f•~-Cc._,<,~-~
1
_,k~·:._c ,(Lf~c-· _L:~,;=rl J~~· c-/ i <.., L'f c,; .r.::.JL •. c(_L,<,_,,,L,''-'L~"L.f~,-~L.,"'"·~'->-L''-''-'LCC-"~'~'-L·L' L' L' -L.L~-~1.,;_,_, l✓L .. L'L·-·~,_,/~k~-~'L'cC--"ic_
I I
800~3\0 moll y Olu. Sollc11 70]00 050 mo/I Ag -SJJur 1 011 ug/1
COO High 340 mg/I rtuo1ld•. o~ 1 moll Al · Ali,mlnum I 1 0 !!. ug /J 01ganopho1p/':01u1 ,a,llcld11
COO lo• "' mg/I
,/ Co//lorm:I-IF F • c,J ]1616.(/00 /IOOml
H ■r<ln•u:To1,1 000 mo/I
H11e1na11 (non-cub) '" mg/I
V •• -B11lum ·1001 G9n """ C• • C1ldum . " mg/I Acl<l H11dlol<l11
Col!lorm:I-IF T 011 I ll~O• / 100ml Phanol, 32 7 JO VO// Cd • C1Clmlum 1027 uo/1
TOC 6110 mg/J Sp•clllc Cond. " uMho1/cm 1 Ch1omlum:Tolal \OJ• u.i/1
T urb I di ly " NTU Sul I ■ 11 '" mQ/1 Cu -Copp11 1 0 4 2 UQ /I Acid £1tr1ct1DI• Qrg1nlot
Su!lld1 '" mg/I Fo • Iron 10•~ uo/1
\/ Hg -IJ•fC:U<y 11000 -:,..Jq UQ/1 X Purg.,DI, 0101nlc:1 ('w'OA borti.J
pH ~ OJ unlu K -Pou11lum Ill} ,ng/1
Atk•llnlly lo pH~-~ "' mQ/J
Alk•llnlly ID pH I.J • 16 mg/I
Caibon11, .. ' mo/I
_Blc:ubon,I• . " mg/J
Aruntc:loUI l 00 2 """
\( NHJ .. N 6 l 0 0,94 mQ/1
T KN .. " '" mo/I
Mg -IJ1gn•tlum 1111 mO,O
Mn, M,n1,11n,11 1056 ug/1
"· Sodium '" mg/I
"' NI c ~ t I 1067 ug/1
)( Pb Lt1d IO~ 1 '10 ug/1
1,2 • OID1omo11h1na {£011,l,: ~{;,--,:·~.-;:,; :_:· ,.'\
.\i.., \·{ ,l!-~1 \;\\ r .J •·~• I;] j
1---+----i';~~"'\"";_·.~~~·--_: --_--_._· -----=-=--'l' ;:;.,;
; C,\. "., P. lS~
y, ......
C11bon dlo•ld• ◄05 moll )( N01-.N0311H '" c; 4, mg/I s. S•l1nlum 1 I ◄ 7 ug /I
Ch!olld• 11~0 moll P:Tolll •• P 685 mo/I Zn line: 1097 UQ /I '--\;1y~·-..... ,·· r.u N-, 11.,"' / ~•"-I .. \, •••'
Ch1om!um;Ha1 I OJ 2 UQ /I I I•••--
Color:11,.,. 80 Pt·Co
Cy• nl <l• "" mo/I
Lab Comment&:
'' (, .
j
GW-!>-1 REV, !l/90 for Dlssolvad Analysis -submli llherod sample and wrile "DI"" !n block
J Whtte Copy• Oroundwalor Con1ral Oltlca Yollow Copy -1.· ' ,naJ 0/llc-O Pink Copy, C-Onlral flk11 Goldenrod C<lnv. I •h
LAB HO. 3G~02.
REPORTED BY u
· CHECKED BY .
REVIEWED BY 0,/(J , '
SAMPLE TYPE: WATER
CASI VOA TARGET COMPOUND
15-35-4 1,1-Dichloroethene 0,15
75-09·2 Methylene Chloride 0.25
156-60-5 trans-1,2-Dichloroethene 0. 15
15-34-3 1,1-Dichloroethane 0.25
590-20-1 2,2-Dichloropropane 0.25
156-59-4 cis-1,2-Dichloroethene 0.25
61-66-3 Chloroforn 0.25
14-91-5 Bromochlorouethane 0.75
11-55-6 1,1,1-Trichloroethane 0.25
563-58-6 1,1-Dichloropropene 0.25
56-23·5 Carbon Tetrachloride 0. 15
101-06-2 1,2-Dichloroethen, 0.25
19-01-6 Trichloroethene 0. 25
18-81-5 1,2-Dichloropropane 0.25
15-27-4 Brouodichloromethane 0.25
14-95-3 Dibromomethane 1
10061-01·5 cis-1,3-Dichloropropene 0.25
10061-02·6 trans-1,3-Dichloropropene 0.25
19-00-5 1,1,2-Trichloroethane 0.25
121-18-4 Tetrachloroethene 0.25
142-28·9 1,3-Dichloropropane 0,25
124-48-1 Dibroaochlorouethane 0. 15
106-93-1 1,2-Dibroaoethane 1
lOB-90-1 Chlorobenzene 1. 2 5
630-20-6 1,1,1,2-Tetrachloroethane 0. 2 5
15-25-2 Bromoforu 0. 5
19-34-5 1,1,2,2-Tetrachloroethane 0. 15
TQL· Target Quantitation Liait-subject to
change due to instrument sensitivity
T· Tentatively Identified, not confirmed
B· Estimated Value
EHNR/DEN LABORATORY
VOLATILE AIIALYTICAL REPORT
ANALYSIS RESULTS
SUPERVISOR~ DATE
ENTERED BY . -
CHECKED BY
CASI VOA TARGET COMPOUND DETECTED
u 96-18-4 1,2,3-Trichloropropane 0. 2 5 u
u 108-86·1 Broaobenzene 1 u
95-49-8 2-Chlorotol uene 0.25
1 . 6 106-43-4 4-Chlorotoluene 0.25 u
541-13-1 1,3-Dichlorobenzene 0.25 0. J 8
2. 3 106-46-1 1,4-Dichlorobenzene 0. 2 5 4. 8 3
u 95-50·1 1,2-Dichlorobenzene 0. 25 4. 2 E
u 96-12-8 1,2-Dibrouo-3-Chloropropane 1 u
120-82-1 1,2,4-Trichlorobenzene 0.25 u
u 81-68-3 Hexachlorobutadiene 0. 25 u
u 81-61-6 1,2,3-Trichlorobenzene 0. 15 u
u 1634-04-4 Nethyl-tert-butyl ether 5 u
0 . 2 5 11-43-2 Benzene 1 2 . 3
u 108-88-3 Toluene 1 u
100-41-4 Ethyl benzene 1 u
108-38-3 u,p-1ylenes 2 2 . 1
u 95-41-6 a-Xylene D
u 100-42-5 Styrene u
u 98-82-8 Isopropylbenzene u
u 103-65-1 n-Propy !benzene 1 u
u 108-61-8 1,3,5-Triuethylbenzene 1 1 B
98-06-6 tert-Butylbenzene 1 u
u 95-63-6 1,2,4-Trimethylbenzene 1 u
5 . 5 135-98-8 sec-Butylbenzene 1 u
u 99-81-6 p-isdpropyltoluene 1 u
u 104-51-8 n-Butylbenzene u
u 91-20-3 Naphthalene u
Other purgeables detected Detected
(up to 10 highest peaks) ug/1
BIGHT UNIDBNTIFIBD PEAKS DmCTED BY
u-Samples analyzed for this compound but GC/PID.
not detected
H-Saaple not analyzed for this compound
D· Detected below quantitation liait
M-GC/KS Analysis performed
COKMRHTS:
.V d I U I I II ci, LAO NUMBER 8 ~-")(~ .~-70 ~3 Department of Environment, Health, and Natural Resources c__ / I j /1 '.2 o C\C:
· · f E · IM t DATE RECEI~~ -,+---'l[!~-t--:l.,__:__~)T1me .D . ) ,, D1v1s1on o nv1ronmenta anaJemen l. 2:, r ~
Groundwal0r F1eld/La.b Form noc'd by -~ 1 rom Ou~)
1'<11 U I l II
Aoporl to: ARO, ARO, WaRO, WiRO, cHAlt!JJf Evld§1igov 0 0 fhe I --------:;::,:------,~=---(}7f; li:f
WSAO, Kinston FO 01t1or
Shippod by: Gus. ~. Olhor
COLLECTOR(SJ:fu'/./\,,, lfr){j (ft,,
I •
FIELD ANALYSES
DATE
Ow nor
~ ROUTINE □ EMERGENCY
TIME lFoO PURPOSE: BASELINE,
C / _ ) , ( f: } '!-C. l k / / ,J ,.-
I
DATA ENTRY BY: --'t,-,~-~ CK: V\ 1 ~
DATE AEPOR TED: __ G~3_6~/_f_J __ ' ___ _
COM PL A I t/T, COMPLIANCE,
(cl1cJe on•)
LUST, OTHER
--1--~✓ }(_
PH400 Spoc. Cond. g-4 __ a1 2s 0c Locarlon or sire Jill 6 1993
Tomp.10 oc Odor Dus c r I pt ion o I s11111p Ii no ~i o In I ~ __ lk~~-~·j._·•~L __ -~l-~~-'~,~-~-,~c'..'S(~---~f.~3~/ "---~' ,~·~,~-~~--· ___________ ,_·_-_________ _
Appouranco Taslo
Field Analysis By:
Sampli nQ Mo I hod
Aornarks I
I nforve f[)HS:Jid! GU~l I t<UL tlRANCH (pump, bollor,
.(' I &V -!.t:. 1
etcJ
>t ... r < c..,,(
__ $amplo
/,_;c; I I e.•·
(pumplno llmo. air lomp. ale.)
LA0Of!ATO11Y ANALYSES -
-~J~·'7~r_',7/l"J)~(L,~•'~•c'-•, __ C,~t,~ fc'••L/-l:fJC-'-[ __ -"/'L•,O_,__:rL1.lcic.'_t-.!.-~lc_· <SJ..£..<'Lfi ________________________ _
BQL)~ 'IO
coo Hlon '"
COO lo• '" '
Collro1m:UF F•c•I J 16Hi
Co11101m:1-1r To t•J J l!>O<f
Toe 6eo
T111t>ldft1 "
PH ◄ 0 3
Alk a llnl ly lo DH ◄.5 ...
Alk•llnllr IO pH '·' .. '
Caibon,I• . "
Blca1bon1t• '"
Arunlc:101,I 1002
Carbon dlo,lde "'
Chlnrhh IHO
Chromlvm:th• 1032
Color:Tr.,. ao
c,,ntd• l>o
Lab Commenla:
ow-~ REV. ll/90
mo/I X oru. Solid• 10300 ? mg/I Ao· Sllv•r 1011 uoll
moll fluorl(h '" mo/I Al • Alu•mln"-'m 1 I 0$ . UQ/1
mo/I H•Hln1u:Tol•l 000 moll X •• · 811lum·100.7 rs .,,,,
/ I UOmJ Haraneu (non-carb) ,., moll c, c,1clum 111G mg/I
1100ml Ph•not1 l 2 1 JO """ Cd C1dmlum 1021 \lg/I
moll Sp•clllc ConJ. " ul-lho•/cm 7 Chrom!um:Toul 1 0 J ◄ llQ/1
NIU Sull • 11 '" moll Cc C:opp., 1 0 ◄ 2 llQ/l
Sullhll I '5 mo/I ,. Iron 100 uo /I
X Hg • u.,,u,1 , 11100 L D ·-:c-l uo /I
11ntu K • Po1111lum IIJ7 mo/I
mo/I Mg • U1on•1lum 1117 mo,,
mg/I I.In -IJ1nv•n••• 1056 uo/1
moll No · Sodium '" mo!/
mo/I X: ""' .. H 6 10 I). 07 mg/I "' • NI ck• I I 06 I . U(,1/1
""" TKN " N '" mg/J V PO l • ad 1 0 5 I 2.10 uo/1
mg/I .x NOJ "'N03 •• H 6JO r), 0/ mg// . s, Selenium I 1 4 7 uo /I
mg/I P:lol•I •• f' 665 mQ/1 '" line 1097 \IQ/I
"0 It
Pl-Co
-moll
_For rnssoivad Analy&i6 -submli llhorod sample and wlile ·01°-· 1 block
White Copy -Oroundwaler Conlral Olllca Yollow Copy-h _ ,nal Olllco Pink Copy -C-Onlral Flklt
o,i;,-.nochlo,ln• ,.•11Jclde1
0101nopho•11r:o_ru1 ,,,nc_ld••
Acid Ht1dlclde1
Be1, I ,..,..,,,.1 E~Lr1c11bl• 0,, ... 1,,
I. 2 • Olbromo~ lhene {EOB)
I /
. LAB HO, JG 703
RBPORTED BY
CHECUDBY ~
REV I BWBD BY ~
SAMPLE TYPE: iATBR
CASI VOA TARGBT COMPOUND
71-35-4 1,1-Dichloroethene
75-09-1 Methylene Chloride
156-60·5 trans-1,2-Dichloroethene
75-31-3 1,1-Dichloroethane
590-10-7 1,1-Dichloropropane
156-59-1 cis-1,1-Dichloroethene
67-66-3 Chlorofon
71-97-5 Bro1ochloro1ethane
71-55·6 1,1,1-Trichloroetbane
563-58-6 1,1-Dichloropropene
56-13-5 carbon Tetrachloride
107-06-1 1,1-Dichloroethane
79-01-6 Trichloroethene
78,87-5 1,1-Dichloropropane
75-17·1 Bro1odichloro1ethane
71-95-3 Dibro101ethane
10061-01-5 cis-1,3-Dichloropropene
10061-01·6 trans-1,3-Dichloropropene
79-00-5 1,1,1-Trichloroethane
117-18-4 Tetrachloroethene
141-18-9 1,3-Dichloropropane
114-48·1 Dibro1ochloro1etbane
106-93·! 1,1-Dibro1oetbane
108-90-7 Cblorobenzene
630-10-6 1,1,1,1·Tetrachloroethane
75-15-1 Bro1ofor1
79-3!-5 1,l,1,1-Tetrachloroetbane
0,75
0.15
0. 7 5
0 .15
0 .15
0 .15
0.15
0.75
0.15
0.15
0,75
0.15
0.15
0.15
0 .15
1
0 .15
0. 25
0.15
0.15
0 .15
0. 7 5
1
0.15
0.15
0. 5
0. 75
TQL· Target Quantitation Li1it-Subject to
change due to instru1ent sensitivity
T· Tentatively Identified, not confiraed
B· Estiaated Value
BHKR/DBH LABORATORY
VOLATILE ANALYTICAL REPORT
i\NALYSIS RBSULTS
SUPERVISOR~ DATB .::,-:W . ,
BRTERED BY / ,.7,
CHECKED BY f )'.:'.'.)
DBTEC1BD CASI VOA TARGBT COMPOUND DBUCTBD
u 1 u 1
u 96-18-1 1,1,3-Trichloropropane 0.15 u
u 108-86-1 Broaobenzene 1 u
u 95-49-8 1-Chlorotoluene 0.15 u
u 106-43-4 4-Chlorotoluene 0,15 u u 541-73-1 1,l-Dichlorobenzene 0.25 u
u 106-16-7 1,4-Dichlorobenzene 0.25 u
u 95-50-1 1,1-Dichlorobenzene 0.15 u
u 96-12-8 l,l-Dibro10·3·Cbloropropane 1 u
u 110-81·1 1,2,4-Trichlorobenzene 0.15 u
u 87-68·3 Hexachlorobutadiene 0.15 □ u 87-61-6 1,1,l·Trichlorobenzene 0.75 u
□ 1631-04-1 Hethyl-tert-butyl ether 5 □ u 71-13-2 Benzene 1 u
0.31 T 108-88-3 Toluene I u
u 100-41-4 Ethyl benzene 1 u
u 108-38·3 1,p-Xylenes 1 u
u 95-17-6 a-Xylene 1 u
u 100-41-5 styrene 1 u
u 98-81-8 Isopropylbenzene 1 u
u 103-65-1 n-Propylbenzene 1 u
u 108-67-8 1,3,5-Triaethylbenzene 1 u
u 98-06-6 tert-Butylbenzene 1 u
u 95-63-6 l,l,l·Tri1ethylbenzene 1 u
u 135-98-8 sec-Butylbenzene 1 u
u 99-87-6 p-isopropyltoluene 1
u 104-51-8 n-Butylbenzene 1 u
u 91-20·3 Naphthalene 1 u
Other purgeables detected Detected
!up to 10 highest peaks) ug/1
OH! UNIDBNTIFIBD PBAK DBTBCTBD BY
u-Saaples analyzed for this coapound but GC/PID,
not detected
H· Saaple not analyzed for this coapound
D· Detected below quantitation liait
H· GC/KS Analysis perfor1ed
COMMENTS:
,._,,__,Vii I I
OUAO r,o 1
' ,,. ,_, '-'. C ,_,
/r-; ~-/.-') ,,;;-SERI Al NO.
LAB NUMBER 8 ,~)\ ~, ,,,_) /'--j Department of Environment, Health, and Natural Resources _q__;;y_-::1,_q-~ . L(: C'C' D. · · f E ' J M DATE RECEIVED-•. ") Time · _ , .-' 1v1s1on o nv1ronm_enta anagement .D; ~;';:;">, LAT. _______ LONG.
WaRO, WiRO,
Groundwater Field/Lab Form Rec'd by.) :=:> From: Bu~ ':; f\l N i~ f"B '~T«lfl1V , } iH" ;\/:I 'i .;· ·L.-r C\_i:. ~ _; 't.)-\.:: K.rJ ... SAMPLE PRIORITY : ..
Other
DATA ENTRY BY: WSRO, Kinston FO Olher '
Stiippod by: Dus~' Oltlor ROUTINE 0 EMEnGENCY
~ ~ 3/J/CtJ DATE REP OR TEO:--~'--'--------:.'
COLLECTOR(S): o::,?,:, /(-{(' DATE r~ h.~ (1/3 TIME Ii .C,j PURPOSE: BASELINE, COMPLAlrn, COMPLI ANGE, LUST, OTHER
FIELD ANALYSES
pH400 ___ Spec. Cond.94 __ at 2s0c
_Temp.10 ____ 0 c Odor _______ _
Appearance _______ Taslo ______ _
Field Analysis By:
LAIJOf'lAlOllY ANALYSES
80D!,310 mg/I
COD Hloh J, 0 moll
COD Lo..-3J!i moll
X Collform:L4F F ,c1 I 31616 ..c_ I / I 00ml
Colllorm:L4F To1 ■r 31!:io◄ 1100ml
TOC 680 moll
Turbldlly 76 NTU
pH ~ 0 J uni I•
AIJ.:.1llnlly lop H ◄. 5 "' mg/I
Alk1ltnl\y 10 OH 8.3 "' mg/I
Owner 'Jj \ ' I Oi· ,,. ,, /4_, (,,. 1-.> ,::.i F ' l. ·" A,1
Location or sile ·· t/ ,:-7 .5,:
Descriplion ol sampling point
Samplinp MoltlOd
Remarks
Dru. solid ■ 10300
FJuorld1 '" H1rdn,u:Tour ,oo
Hardn,11 (non-cub) 1102
Ph1nol1 32730
Sp,clllc Cond. " SuJl■I■ 945
SuJIJd, "s
mo/1
mo/I
moll
mo/I
UQ II
ul.4ho■/cm 7
mg/I
moll
i
.1·.1-,-
z~{t /'/
Ag -Sll'f■

r

1077
Al -Alumlnum I 105
•• -Barium ·1001
C1 -C1lclum 1116
Cd -Cadmium 1027
Chromlum:Toc■I IOH
Cu -Copper I 0-4 2
F■ -Iron 10◄ !,
Hg -L4trcu,y 11 goo
K -Pot■nlum 1137
1.4g -L41gn,1lum 927
l.ln -M■no■n••• 1055
(~ircia;·OM)
_:Li(. Sf« fou, 11 r·
C..? r{ ,-f',·•r -!. /-~··'.
(/ :.~.·'::.1,:z: i Oft"
(pump/no limo. air lomp, etc.)
uo/1 Org1nochlorln• l-•11lcld,1
ug/1 Oro1nopho1pho:u, P•llloldll
ug/1
moll Acid H11dhild11
uo/1
uo/1 B 111 / N1u1r1I E•lncl1bl1 Org",nlcu
uoll Acid E•tr1cl1bJ1 Oro1nlo1
ug/1
ug/1 Purg11bl1 Oro1nlc1 {VOA bo1tl1} -mg/I
mg/I 1,2 -Olbromo■lh1n1 (EOB)
ug/1 _..,,,:-::;1,?W1. ' moll N■ -Sodium 9211 moll .,.,.-,, \c:-r1 t:.J~l-J.:'\ ,·~ l !. OJcubon•I• , " mg/I NH3 .. N 6 J 0 G,D:, moll NI · NI c ~•I 1 0 6 7 uoll \•,<~--ArunJc:Tout 1002 uoll TKN .. N 625 moll Pb L11d 10!1 I uo/1 ,Li,~ ,p;IJ) 1 i 129; Carbon dJ01Jd • ◄ O!> mo/I X. N02 -t NQJ II N 630 I I, mg// s, S1!1nlum 11 ◄1 uoll
._,.,. __ . .
ChJnrJd, g◄o mg/I P:To111 u P 66!, moll '" Zinc 10n ug/1 r-r,f'\: u·.in\;:.i'!lR si:" .. ., TiOH ChromJum:Hu UD /J ~· -r.t\l ;::'!~~ ~· '
1032
" -.. -Color:T,,..., eo Pt•Co
Cy,nl(h 120 moll
Lab Commenls: 3-tS-jo
V
GW-54 REV. 9/90 For Dissolved Analysis -submll lllterad sample and writo .·-•·,· 1n block
White Copy -Groundwaler Cenlral Olllce Yellow Cop) · .aglonal Olflca Pink Copy -Central Flies GolnAnrn<l (',.nnv ~ I i:1h
cour,1 y, ~1:.1 rl'(, //
OUAD Noil/7,1-rJ
: ...
SERI AL NO, . ,, ,-'.> , ,, LONG .. Yt) . .} I?
North Carolina 3f:J-"p
LAB NUMBER 8 :\C-:T .~ '.zs() Department of Environment, Health, and Natural Resources ri '-:> 03 ()--,
DATE RECEIVE[)O)'d-:)--1_ Time 1,UC) Division of Environmental Management .L>=
G d F, ld/L b f Rec'd by: . _-:;:, From: Bus~~ roun water 10 a Offi1 .•• -••. ,,:-;-, ~
Report WaRO, WiRO, -,~'.,HA~ ~A Oh EGJi11t,}vY~-~::; ~ \€),~9~3 I :::: ENTRY BY:~'~)~~--CK.,/);; k/ WSAO, Kinston FO Olher _______ _
Shiµpod by: Ou~ Olher ______ _
□ fv1 \\,Mt\ ~ // ( (C-' ROUTINE 16.1 EMERGENCY OATE REPORTE0:-'-)~--'--'1--'µ=-------
COLLECTOR(S): l)l[c tL DATE ?/u/'i :J TIME _(_o_·_. _:.,_'~; __ _
FIELD ANALYSES Ow nor
DH4QQ ___ Spec. Cond. 94 ____ al 2s0 c Location or site
. r:(~~1:>.lf':\
pr;;, in .on cnN1JJ~_ 01\r•.\\Vl
PURPOSE': 'B'ASELINE, COMPLAINT, COMPLIANCE, LUST,
(circle o~)
OTHER _____ _
,,<-(. It /30X .55'7 .S/7 /..-,-u, 1Ie . .J,J-0 ?7
5"./<..~-/dcc,i' Qr? ,-:ft1r t .K'-c, ::.· a../J so,, f(, of S'.,.r'."/....?1-...?
Temp.10 ____ 0 c Odor ______ _ De scrip Ii on ol samp Ii ng po Int _Li ,:c,~'--"""'-'--1-'----ec'<.· ~' ,e,·;;lle,_ __________________________ _
Samplin(I Melhod -:Sr+--Pu n-u? Appoarance _______ Taslo ______ _
Field Analysis By: ____________ _ (pump, baller, 101cJ 7
"Bv ,,.Pel &l-'{fi Remarks
Sample Interval _____________ _
LAIIOnATOl!Y ANAi YSES -
PIPC!Se
;Ji i 1:l Sr-.·;v1;?/.,.l 5 h ,.,f t>rrv•( V / ;/ t t/ { ( /7-;> -/J/f . .:iC/v r
8005 J 10 mg/I V Din. Solidi 70300 1 J.-0 mg/I Ag • SJlur 1077 uoll Organochlorln• P11tlold11
COO HIQh 340 mQII fluortda IIS t mg/I Al -Alumlnum 1106 <'5() ug/1 Organopho1phoru, P11llold11
COO Lo"" l35 mo/J
V Colltorm:l.4f f•cal 31616 ..::._/ J:tlOOml
Colllorm:l.4f Tolal J 1504 1100ml
Hudnau:To111 1100 mQ/1
Hudna11 (non-carbl fil02 mg/I
Phenol, 32/JO ug/1
:v 81 -Barium ·1001 1..~ri 1'/C) ug/1
;,( Ca -Calclum fil 16 J.t+-r5 ;2/ mg/I
x Cd • C■dmJum 1027 ,.'kf' <J [)•OIi
;..;:; t r;"r-Irv r;;i \';.,r-,,_ /l!i '/!:!i ,.,.,,.,£~.;~,:!:{~ If))
TOC 660 mg/J Sptclllc Cond. " ul.4ho1/cm1 X' Chromlum:Tol1I IOH <;~5 ug/1 /li 'fe~u !J~■u.~r.,J_Ex1rJi//b11 Otganlo■
Turbidity 76 NTU Sullale 1145 mg/I X Cu -Copp•f 1042 3? ug/1
Sullld1 745 mg/I >< f• • Jron 10◄ 5 l1)D ug/1
y Hg -l.41rcuq, 711100 I I({) ug/1
pH ~OJ un111 / K • Pollnlum 1137 ,_;;. g-moll ·r 'I\,,
Alklllnlly to pH ◄.5 "' mg/I V 1.4g • l.41gn'1lum 1121 ·I-. 5 moJI 1,2 -Olbromo~lh■n ■ (£08)
Alk1llnlly to pH ,., "' mg/I V Un -l.4ang ■n••• JOSS .~.c., ug/1
Ca,lional• . " mg/I X N ■ -Sodium 8211 :5 .. 3 mg/I
Ulc ■rbon•t• .. , mg/I Nli3 a I N 6 I 0 o. o':) mg/I y' NI • NI ck• I 1067 < IC) ug/1
Arunlc:10111 1002 vg/1 TKN1aN625 mg/I v Pb - l • •d 1 0 S I -z 10 ug/1
Carbon dlo1lda 405 fflQ/1 V NOJ -. N03 •• N 630 1 ".?,, mg/I s, -S•l1nlum 1147 ug/1 /'
Chloflda 11•0 mg/I P:Tol1I 11 P 665 mg/I x '" -Zinc 1091 ,-::)4 ug/1 I/
Ch1umlum:tt•• 1032 ug/1
Colo1:fr,.. 110 Pl-Co
c~•nld• '10 fflQ/1
Lab Commenls; ·-=·-=-=··_:::C;;,,' !./!.!lu:si..L"',:::·,:::--:.....:•;,'3c;,., ~l~~.u.,,-,=1!:l·,(_:
1 ft:-',t:'!./-,'/'---------------------------------~t':-J.,=-,---------
r1/c3¢r'?
GW-5-4 REV. ~ For Dlssolvad Analysis • submit flherad sample and wrile.;~;;v In block
BHNR/DEH LABORATORY
VOLATILE ANALYTICAL REPORT
LAB 110. 3G280
REPORTED BY ~ ;;,,,,,,,, ~ I
CHECKED B'/ tek'~ DATE <i< ~ • 3 I
(Z;<fl__, ·• REVIEWED BY ENTERED BY l CnlCKBD BY W7 tr;.,/
SAMPLE TYPE: WATER AIIALYS!S RESULTS :I
'I
CASI VOA TARGET COHPOUIID TQL DETECTED CASI VOA TARGET COMPOUIID TQc DE?JC?% '
uo 1 uo 1 uo/1 uc/1
75-35·4 1,1-Dichloroethene 0,15 u 96-18·4 1,2,3-rrichloropropane 0.25 u
75-09-2 Methylene Chloride 0,25 u 108-86·1 Broaobenzene u
156-60·5 trans-1,2-Dichloroethene 0.75 u 95-49·8 2-Chlorotoluene 0.25 u
75-34·3 1,1-Dichloroethane 0.25 D 106-43-4 4-Chlorotoluene Q.25. u
590-20-7 2,2-Dichloropropane 0,25 u 541-13·1 1,l-Dichlorobenzene 0, 2 5 D
156-59-4 cis-1,2-Dichioroethene 0.25 D 106-46·7 1,4-Dichlorobenzene Q.25 0. 36
67-66·3 Chloroforn 0,25 u 95-50·1 1,2-Dichiorobenzene 0,25 D
74-97-5 Bromochloromethane 0,75 u 96-12-8 1,2-Dibromo-3-Chloropropane 1 u
11-55-6 1,1,l·Trichloroethane 0,25 u 120-82·1 1,2,4-Trichiorobenzene Q.25 u
563-58·6 1,1-Dichloropropene 0.25 u 87-68·3 Hexachlorobutadiene 0. 25 u
56-23-5 Carbon Tetrachloride 0,75 u 37-61-6 1,2,3-Trichlorobenzene 0.75 u
107-06-2 1,2-Dichloroethane 0,25 u 1634-04·4 Hethyi-tert-butyl ether 5 u
79-01·6 Trichloroethene 0,25 D 71-43·2 Benzene u
78-87-5 1,2-Dichloropropane 0,25 u 108-88·3 Toluene u
75-27-4 Bromodichloromethane 0,25 u 100-41-4 Ethyl benzene u
74-95-l Dibromomethane 1 u 108-38·3 .,p-Xylenes u
[ .-· 10061-01-5 cis·l,3-Dichloropropene 0, 2 5 u 95-47·6 a-Xylene ;j
10061-02-6 trans-1,l·Dichloropropene 0,25 u 100-42·5 Styrene u
79-00·5 1,1,2-Trichloroethane 0,25 u 98-82·8 Isopropylbenzene u
127-18·4 Tetrachloroethene 0,25 D 103-65-1 n·Propylbenzene u
142-28·9 1,3-Dichloropropane 0,25 u 10S-67·8 l,l,5-Jri.ethylbenzene u
124-48·1 Dibromochloromethane 0, 7 5 u 98-06-6 tert-Butylbenzene u
106-93-4 1,2-Dibromoethane 1 u 95-63·6 1,2,4-Trimethyibenzene u
108-90-7 Chlorobenzene 0,25 u 135-98·8 sec-Butyibenzene u
630-20·6 1,1,1,2-Tetrachloroethane 0,25 u 99-87-6 p·isopropyltoluene u
75-25·2 Bromoform 0, 5 u 104-51-8 n·Butylbenzene u
79-34-5 1,1,2,2-Tetrachloroethane 0, 75 u 91-20-J llaphthalene
TQL· Target Quantitation Limit· Subject to Other purgeables detected Detected
change due to instrument sensitivity lup to 10 highest peaks) ug/i
T· Tentatively Identified, not confira,d
B· Estimated Value
U· samples analyzed for this compound but
not detected NO VOLATILE ORTGAlliC COHPOUIIDS
N· sample not analyzed for this compound QUA!ITITATBD BY GC/PID,
D· Detected below quantitation limit
H· GC/HS Analysis performed
COMMENTS:
C
LA l.
I NO. Lyt·/,, _,;:
North Carclina
SERIAL NO.----
LONG. _____ _
LAB NUMBER 6 ~~ Ii~ 5
Department of Environment, Health, and Natural Resources / . 9 /'c:'
DATE RECEIVED U+L-4--1--~..+-Time ::.J. •--:::;;).-
DivisiOn of Environmental Management/ T · •
Groundwater Field/Lab Form REcr::~~rrn DS From Busev
/ -!
Report to: ARO. FR0,\~_5..0. ARO, WaAO, WiAO, r\-ffi~uofR£i\i£10D'( {mi'\ ~:~JteNTAY BY. V£-cf-19-
WSRO, Kins1on FO Olher ________ _
[S ROUTINE O EMERGENCY P0Lc~f<f~0t ~~A'.rftJED: (--£!-~
Shipped Oy; Bus. Courier, Olher _______ _
COLLECT OR ( S); __ ··-~/'~--;~/~:•.~, ~-' ·_•,_/ __ DATE
FIELD ANALYSES
PH 4 oo ---Spec. Cond. 94 __ at 2s 0 c
1emp.10 ____ oc Odor ______ _
Appearance _______ Taste ______ _
Field Analysis By: ____________ _
LABORATORY ANALYSES
BOD!, J JO mg/I
COD HIOl'l HO mg/I
COO Low JJ!, mg/I
Colllorm:I.IF Fecal 3 16 1 6 1100ml
Colllorm;MF T OIi I 3 150-t /\OOml
TOG 680 moll
TurOldlly 76 NTU
PH 4 OJ uni 11
Alkallnlty 10 pH 4.5 <JO mg/I
A 1 ~ &!lnl tr JO PH 8. 3 4 1 5 moll
C11tion ■

1
•

... mg/I
Blcubon,1, ... moll
Arwnlc:Total 1002 UQ/1.
Carbon dlo:llO• -405 mg/I
Chlotld1 i-40 moll
Chromlum:H■

A

1032 ug/1
Color;Tr~ •• Pl-Co
Cy1nl01 720 mg/I
Lab Comments:
PURPOSE: BASELINE, COMPLAINT, COMPLIANCE, LUST, OTHER
(c:i,chl on.el '
/41(
owner __ .!..1"-( 66"as.· ,,..a,P:..,..__.J.,,«:::::_g_o!_«~,1..:'fi.-.,;,:,., __ 41'.:../.c:,,_.!_I .1'/ _ _,{~'JLOLl.\'.__;J!..cc?;e-:.:'-0:·_..:-"::.·-'/-r".'-' .:.i;...2.,..,u~·.!..· .!..; :..,1 r:..._ __ ....=S::...2='5::..· _·,:6_· -'-Y_.9:_.:.·~L./
Loe a Ii on or si 10 ( 'I mrfP r &/I ~-fr;.. / .. cJ'. .S,~._,,1 tl-
Description of sampling point Pi.I a/: We//
Sampling Method
Remarks ; -• I ,-·.-,· :.' ,• I' '.' . -;.,_. ' '' .. -
'"T'.' .. r ; . . -:.............._-I ~--_·c..,-~ (pumping time. air lemp, etc.)
-( /
Olu . Solidi 70300 mg/l K Ag· Slln '"" .C5,0 ""11 Oro1nochlorlM l'11Hcld11
F1uo ride 95 1 moll y' Al • Alumlnu.m 1105 Lf'',I\ ug/1 Org1nopho1phoru1 P11lloldll
Hatd r..u:Total 000 mo/I ,/ 81 • Barium 1007 ~';< ... ,1
Hard nan (non-cub) 002 mo/I .. / c, • Calclum 016 / I mg/I Acid H1rdlcld11
Pho nol, J2730 uo/1 x Cd • Cadmium 1027 L.. '1.0 ,.,1
Spo clllc Cond. " ui.11'101/cm 1 < Cl'lromium:To11I 1034 L ::,,=;-ug/1 B••• / N•uHII E11nclabl• OrgaAICI
Sul! l I• 9-4 5 moll < Cu • Coppu 104 2 '7, '7 ug/1 Acid E.11rac11bla o,aanlca
S ull Ida 745 mg/I < Fa • Iron 1045 ,(&q\ ug/1
I< Hg • Marcufy 7 1900 L li\,..J"'\ ug11 IX Purgaabla Orgal'Mca (VOA llQtlia)
\( K • Po11uJl,lffl 937 . I,{,, ,ng/1
< tr.lg • t.11gnul1,1tJ1 927 .-,_=, m.,J 1.2 • OlbrQ,noalhan• (EOI)
tr.In • t.11n<,11n.11 1055 IC::. --,\ .... ug/1
' N• -Sodium 929 u_e, mg/I __.,-:')G.)<;"'?"7\,1(--. ,,
u N 610 mg/I ,\.,... NI -Nickal 1067 LIO ug/1 (ri'll~l(,;Jt,nJl 1'/ Jit lt\\
TKN 11 N 625 mg/I \' Pb • LI Id 1051 < 10 UQ/1 Iii~" 1111
<tN0311N 6JO s, • s,1,nium I 14 7 ug/1 <.:>:.> ··•-II , P. 1QQ) ·-mg/I
P:To \al II P 66S mg/I X Zn· Zinc 1092 L l" . ' ug/1
GROIIN.1WUFP ~!'."Til'HJ
RAI J:I~~.: Nr
GW-54 RE090 For Dissolved Analysis -sut,n.(: lered sample and w\.,..>01s· in block
Whn• Copy. Groundwaior co'nir~I Olficq YslloW Copy, ROQlonal Ottic,, Pini< Copy. C..nlral Flie. Goldenrod G<>py. Lab
I
[UNO/DCM l.AQOU.A.TOUY VOLJa.Tll CC ANALYTICAL OCPODT
c,.;su ',iC1 A T ar1,1':'t C(lrnoound TQL
ug/L
75-35-4 1 . i -Di.:;i1lorvi:-H1>:n~ 0.75 ------------------75-0"-2 M,:-ih1.Jle-r1,:-Chlot·l':1,:-0.25
SUPEl'\%0F:
rATE
Ei'ITEREl.o B·,·, .-.f.--'-'-'-'4"-""-
CHEC!'.ED BY
Ai·IAL'i'SIS F:[c:IJL TS
C1Jr1,:; I c·cV -/\~
Detected M'::I
IJQ il
u 96-1 t:-4
LI 108-86·-1
VO A T c1rget C,Jrr,p,:iurtd
1 2 ,3-Trl,:;:hlor1:,or"ooc1ne
8romob€'nzie-ne
156-6(1-5 tr c1ns-I .2-Dlch loroethe-ne 0.75 u 95-4 9-812-Ch loroio luene
7~•-34-3 1 1-Dldih::,rodh.ane 0 --.~ .£.J 0_6:,
590-21}-7 2 ,2-Dlch l◊r·o1:wopan.::-0.25 LI
i56-59-4 i;ls-1 ,2-Dlchloroet~,en~ 0 .-.,::: .£.J u
E,7-66-3 Chlr:,roforrri 0.25 IJ
?4-':17-5 8romcu~hlor,:imeth;,n':' , 0.75 I_I
____ 71-55-~, 1 . l-Trl.::hl0r0i::--th>:1nt2 0.25 u
5E,3-:",8-t,! 1 , l -Dichloroprop0ne 0.25 I_I
5E,-:?3-5IC,3rbon T ':'fr ach loridt? 0.751 u -1.Lt7-·06-2 i .2-Dfoh1vr.:.,ethc1nt' 0.25 u
79-01-b T t"ic.h loroi?th':'ne 0.25 0.29
78-87-5 1 ,2-0ich lor"ODfOl)drlt' 0.L51 u
75-27-4 Bromodic:h lor omt>lhane 0.25 u
74-95-3 Dibromome-thane-1 u
0061-01-5 ,:;is-1 3-Dichloropropene 0.25 u
0061-02-E, lr.:in~-1 .3-Di::-.h1crorwope-ne n ,-,i:::--.......... 'U
79-00-5 I 1 2-T rich loroeihane 0.25
127-lS-4 T etr act,loroe\hene 0.25
142-28-9 1 3..:Dich J,:ir0pr,:ipa~ 0.25
124-48-1 D ibromoch loromt'than~ 0.75
106-93-4 1 2-Dibr orc,ot"thdne 1
108-90-7 Ch l,:,robe-nze-ne-0.25
630-20-6 1,_1.1 2-T t"t.r-achk,roethane 0.25
--
75-25-2 Br◊m•)form I
79-34-5 I .1.22-Te-trdchloroethar,e-0.75
TQL-+.<lrge-t q•.1antit~h,n limit
T-te-nt.atlvE-ly 1de-nt1flt"d compour,d
E·· estlrrr..:1te-d ,..-alu':'
U--:-:0rnpound ~,., a'E. e1n,1 h~ ZP'1 for but
riot detected
~l-not an<J ltJZl:'d for this compound
[>-detected below quanli\ati,,r, limit
MS->:=GC/f-·JS on<1iy.;is pt-t·fonrlt'd
D
TQL 5ub ject to change due tc instrument 5ensiHvit1J
cor-1MEIHS :
u
LI
u
LI
u
u
LI
u
106-43-4 4-Ct-.lvroto lut<nt'
541-73-1 1 3-Dich lorobe-nzene-.
106-46-7 1 4-Dlch lorobt'nzt>ne
95-50-1 j 2-Dich lorobE-nz::E-r,':'
96-12-8 1 .2-Dibromo-3-Chkwoprop,Jn':'
i 20-82-1 1 2 4-T ric:h lon:,be-nz-:--nt'
87-E,f;-3 HE-xachlor1:ibutadi>?ne
t:7-61-6 1 ,2 3-Trichlorobt:'nzene
lE-c:4-04-4 Melhu Hert-bu\u l ether
71-43-2 Benzene
108-88-3 To lue-nt'
100-41-4 Elhu l bencene
108-38-3 m ,o-X~lenes
95-47-6 o-X~ lt?ne
100-42-5 Sh1rent'
98-82-8 lsonroou !benzene
103-65-1 n-Proou lbt-nzent:'
108-67-8 1 3 5-T rimelh•i !benzene
98-06-6 terl-Butu lbenzer,e
95-€-3-6 1 2 4-T rimt-thu lbenzent'
135-98-8 sec-But1..1 lbenzene-
99-87-6 p-lsopror.u lto luer,e
104-51-8 n-Butu lbffize-nl!"
91-20-3 Naohlha lene
NO VOLATILES DE1ECTED
BY GC/PIC>.
TCiL
ug/1
0.25
1
0.25
0.25
0.25
0.25
0.25
I
0.25
0 -:;,c ---0.75
e c•
1
I
1
1
I
1
1
1
1
I
' I
1
1
1
(one
C),:,tedt>d
'..!Q /L.
D>?t':'i:-:~'!',j
U<Jil
MS
u
LI
u
u
LI
u
u
LI I
u
IJ !
u I
u
LI
u
u
u I
u
LI
LI
u
LI
u
IJ
IJ
u
u
LI
COUNTY
OUl,C• r-JO. SERIAL NO.
LOi./G.
North Carolina ~/1-{:)..;J.4 LAB NUMBER 8 l5 Department of Environment, Health.and Na.tural Resources J''I~ qi C¥'J~
. . . . 0 AT E R E CE I V E O -----,./•---,.-----T I me :Li.._.L_ D1v1s1on of Environmental Mana~~f" J:' 1, 1 5 1
Groundwater Field/Lab For!nlL..,_,, __ ,' >! [{)iec'd by: D From Bus~
~,
Report to: ARO, FRO.~~-'RRO, WaRO. WiRO, CHftJ,~~iGf fRld~,Tf)nyJAN 1~ :::·; ENTRY BY: lUv CK:~
WSRO, Kinston FO 0 lh er ________ _ o ROUTINE o EMERGfilJ_~\:iTION CO~liilfl'\JH' REPORTED:_~/--8~-_,_C/~'V~--·----------:, Shi-pped by: Bus(Courie_i,' Other _______ _
~< COLLECTOR(S): I __µ/J,i / ,-,-
FIELD ANALYSES
DH4 00 Spec. Cond. 94
Temp.10 oc Odor
DATE
--at 2s0 c
TIME 3 OS
Owner
PURPOSE: BASELINE, COMPLAINT,
(ctfcJe
/J'O/< d'5·?
s ,['. ;oov
T
COMPLIANCE, LUST, OTHER ..1.f_~:_';_(ic._'_. _/._-_✓0..:·,_,~'-,-, ·-
on.e) :;
5/4 /c,u,llc ,U(" -~f-6 ?-? .~..::r -J ~ --,·-:::1.::
e '' j /~-,:"-(,) So~il_ ~,, s t'. / .? _?'?
c;
Appearance Taste
Location or sile
Description of sampling
Sampling Melhod
Remarks Field Analysis By:
LABORATORY ANALYSES JAN 10
B005JIO mg/I Dlu. Solid, 70300 mg/I .'< Ag • Slt~er 1077 .L$.( l ug/1 OrQ•l').Ps_hj~~•-11•_ !'.•.~llcJg_, •-__ . -..
COD High 340 mg/I Fluorla, 951 mg/I -( Al • AlvmlnUm 1 1 05 ~so ug/1 6rgzJJ~dLP~J/j';tp~~1'11c11t";,'..., I 1Ui'4
COO Lo ... '" mg/I Huan,u:Totzt 900 mg/I < Bz -Batlum 1007 ;;i.-n vg/1 ' IV\Lt.l\:JH, l'I I.,
ColJJorm:MF Feczl 3 16 16 1100ml Huaness {non-cub) 902 mg/I >( Cz • C1lclum 916 '-1"1 mg/I 6cJ.1S.,tt•1.dJ C Id•• . . . Colllorm:MF Toul J1504 1100ml Phenol, J2730 ug/1 / ca -Culmium 1027 cQn ""
TOC 660 mg/I So,clllc Cond. 95 ul.ll'l01/cm.2 < Chromlum:Toi.l 103-4 c:::,5 ug/1 B•u I N,u1tal Ezlracllbl• Orga11J1:t
TurbJally 76 NTU Sullzlt 945 mg/J 1· Cu -Coppu 104 2 IL\ ug/J Acid ExlracUbla Org1nlc1
SullJa, 745 mg/I \' Fe -Iron 1045 .::::::;-:='l'r) ug/1
< Hg • l,hrcury 7 1900 I . '°' UQ/1 'x' Purg,able Org1nlc;1 {VOA bottle)
pH .,, unit• \/ K • Polluium 937 1.0 mg/I
Al~;allnlly !O pH <4,5 «o mg/J ' Mg • M;agnasium 927 Jd mg/I 1,2 -Oibromoathane (EOB)
Alkal!nJly to PH '·' • ,s mg/I y Mn • M1no1n1,1 1055 1<..\0 ug/1
C 1rbon11, .. ' mg/I \• Na • Soalum 929 I "'> mg/I
Blcubonz1, «o mo/I NH3 " N 610 mg/I I-' NI -Nick1I 1067 ,( \U ug/1 SIT,. ~ OAl:'-ANll'C.
ArunJc:Tou! 1002 "'" TKN ;as . N 625 mg/J \ · Pb • L, za 105 1 ..: 10 ug/1 -~N.dl .!"JS: A&:'PORl
c,rbon alox!a, 405 mo11 No2 • N03 as N 6JO mg/I s, -S1l1nium I 1 I 7 ug/1 -. I ' Chi orl a, 9·'° mg/I P:Toar u P 665 mo/I y Zn -Zinc 109:2 ;J,:;;M ug/l . -. V
Cruomlum:H,x tOJ2 ug/J '
Color:True 80 Pt-Co
Cy I nl d • 720 mg/I
Lab Comments: -I J 7 -'1 --
For Dissolved Analysis -subrt_'.,tared sample and ~ .• >rns· in block
Whrte Copy· Groundwater Cenlral Offi~ Yellow Copy• Regional Ottce Pink Copy . Central Flies Goldenrod Copy. Lab
CUNU/D["M LADOU.6.TOOV VOLA.TILt:C ANA.LVl'ICJ..L OLPOUT
1G1224
1:·HU.:f:"'.ff1 8Y
:-~[\11[·,·,IL, 8\'
3/,1 IFLE T,TE: VATCR
, .... , ,,.._,.,..,, ,., .... ,-,r, .;(..•1·1.:.r,v 1-.::-ur:.
[,AT[
C:NTEREL• E:',' -L'CLL'-=""'1
CHECKED E:Y "=c1t,U..:
ANALYSIS RESULTS
T(IL Cone CASu VOA Tan;1E-t Cornpound
ug/L Dtt.eded 11S
uq/L
96-18-4 l -~ 3-Trk:hlorooroodne-
75-09-~1Methwlene Chloride· 0.25 U 108-86-1 Bromoberiz:e-ne
156-60-5 (rans-1 .2-Dichk-roe(hene 0.75 U 95-49-8 2-Chloroto luene
75-34-3 1 1-LJichloroethane 0.25 0.57 106-43-4 4-Chlo.-oto lu;-ne
590-20-7 2 .2-Dichlorooron.,ne 0.25 541-73-1 1 3-Dich lorobenzene
156-59-4 cis-1 .2-Dich loroetr,ene 0.25 D u 106-46-7 1 ,4-Dichlorobenz:ene-
67-f.f..,-"3_. Chloroform D '35-50-1 1 .2-Dichloroben:E-nE-
74-97-5 BromochloromE-t.hano? 0.75 LI %-12-8 1 .2-Dlbromo-3-Chlori:,proD.anl:'
'---' i -55-E-1 , 1 , 1-T,-ioh],)t'Oe.~t"-ho°'· r"-'"---'---'0'-".25 D LI 120-82-1 1 ,2 .4-Trichk1rob1:-n:H1':'
SE.3-58-6 1. l-Dirhk,roo1·01:,-?r1E-0.25 U 87-68-3 He-x.ach lor,:;t.ut :idien,:·
56-2:5-5 Carbon T-etr.:1r::hlorl,je 0.75 U 87-61-6 1 2 ,3-T rir::h lorob1::>n2t?n1:-
j -107-06-:'. 1 ::'.-Dkhlor,:it'lhZJr;t'
,.:-7"-C\1-6 Trichk,r,,ethene rJ .2'5 ! 0 .89
i 62-4-04-4 Melhwl-ted-bul~l fU1t:r
7t-43-2 8.-:-nz:en('
108-88-3 T (tlUt'Ot'
,00-41 °4 Eth1..11 bE-n:N1E-
I 108-38-3 m ,n-Xq lenE-S
95-47-6 o-Xlllt'nt' r
D 0061-0)=5 eis-1 .3-~i)_0ic,·0t:c,lv,c·r.:-o'.l:r,,_r"'opc,·•c.r,,0e_+-"Oc:.2e:5:'....l-___ --1-,cU-1-~ -~"-~---"'-'--'-=--'---
~ 00C 1-02-E. tnr,s-1 ?,-C"ichlorooroot'fie 0.25 U
79-00-5 I , I ,2-T rich lo,·oethane O .25 U
127-18-4 Tt'lrai;hloro~lh,:-ne 0.2:: 0.53
142-28-9 1 3-DiehloroorO"an• 0.25 U
124-48-1 [,iuromochloromethane 0.75 U
1 OE,-93-4 1 2-Dibromoelhdm· 1 U
108-90-7 Chlorobenzene 0.25 LI
~-20-6 1 .1 .I 2-Tet1·4chioroelhane 0.25 LI
LI
(.
75-25-2 Bromoform 1
79-34-5 1 , 1 ,2 2-Tetrachloroethane 0.75
TQL -target. quantltatfon limit.
T-tentatively identiiied compound
E-eshmated valut-
U-compound ,.,., as: .1n.i l\J :r.Pd for but
not detected
N-r,ol .an~ ly :E-d for thfr ~ornpound
(,-dl:'t.ected t-elo'v,r q1JantH.<Jhon limit
i1S-: .. ;:.:QC /i-1S .aria 1y :s:i::. pe-rformed
TOL ::.ubjl!>•::l i,:i change du~ to ;nstrument ::.er.sithity
Cot·IMl:NTS.
u
I 00-42-5 St.4n·ne
98-82-8 1s-oou !benzene
103-65-1 n-Proo1..1 lbenz:ent'
108-67-8 1 3 5-T rimethu lb'?"nz.enl:'
98-06-6 tert-Butu ]benzene
'35-63-6 1 .2 .4-Trimet.h1..1lbe-nz:ene
135-9808 sec-But4lb1::>nzene
99-87-6 o-lsooroou ]toluene
104-51-8 n-8•J~IJ lbt-nzt-r,t-
91-20-3 Naohtha Jene
Olhff punJ<?<Jb 11::>r ( up to 1 0 high,:,st P"dks)
ONE UNID£NTIFIED PEAK
DETECTED Bi' GCIELCD.
FOUR IJNIDENTIFIEu PEAKS
DETECTC:D BY GC/PIU.
i
TCtL
1Jg/l
0 ")<a· _,;_J
1
0.25
0 ~-.L~
0.25
0.25
0.25
1
Q r,t: .L,}
0.2:,
0 75
5
1
I
;
1
I
I
I
1
1
1
1
1
I
I
1
I
I
I
Dt:t.'="ct.e-d
uq/L
D
1.S
0.3
D
5.1
1.3
D
C:.ric
D"t'='('.tl?d
ug/L
•,
U I
u I l
I Li I
LI
1_1 !
u:
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u
State of North Carolina
Department of Environment, Health, and Natural Resources
Mooresville Regional Office
James C. 1\tbrtin, Covcrnor
William \V. Cobey, Jr., Secretary
Mr. Barry Sigmon
Albert F Hilton, Re6"onal 1'-lanagcr
DIVISION OF ENVIRONMENTAL MANAGEMENT
April 8, 1991
A.A.A. Enterp~ises, Inc.
Route 14, Box 350
Statesville, North Carolina 28677
Dear Mr. Sigmon:
RE: Groundwater Sampling Results
Sigmon Septic Tank Service
Groundwater Incident #3422
Iredell County, N.C.
On August 9, 1990 you were issued a Notice of Violation (NOV)
from the Division of Environmental Management (DEM) for violation
of the North Carolina Groundwater Standards ~15A NCAC 2L .0202).
In the NOV you were required to determine the vertical ~nd
horizontal extent of soil and groundwater contamination and to
submit a site assessment report within 60 days of receipt of the
NOV.
On September 5, 1990 I met with you at the subject site along
with Karl Shafer and Steve Clayton from the Solid Waste Section,
Division of Solid Waste Management (DSWM) and Scott Readling from
the Hazardous Waste Section, DSWM. During that meeting it was
decided that you would conduct, or have conducted on your behalf, a
preliminary site assessment which would include the installation
and sampling of two monitor wells per the Groundwater Section
guidelines and the sampling of the ten surface impoundments per the
Hazardous Waste Section guidelines. Based upon the results of this
assessment a determination would be made as to what further actions
would be necessary in order for you to achieve compliance with
North Carolina law. RECEIVED
POLLUTION CONTROL BRANCH
919 North Main Street, i\-loi:m:svilk, NC 28115 • li:k:phom:.70-t-663-1699 • FAX [phone]
An Equal Opportunity Affirmative Action Employer
Mr. Barry Sigmon
April 8, 1991
Page Two
Staff of the Mooresville Regional Office Groundwater Section
received the sampling results for the two monitor wells on March
19, 1991. The results indicate that groundwater at your facility
has been adversely impacted. The following constituents were
detected in violation of North Carolina's Groundwater Standards:
Constituent
1,1-Dichloroethane
Vinyl Chloride
1,4-Dichlorobenzene
Iron
Manganese
Concentration*
1
2·
3
20,000
17,500
* In micrograms per liter
2L Standard*
ND
.015
1 . 8
300
50
ND -Not permitted in detectable concentrations
The DSWM issued a NOV (Docket #91-127) to you on March 26,
1991. In the NOV you were required to-characterize the liquid
waste from and soil underlying each surface impoundment by May 1,
1991. It is our understanding that if characteristic hazardous
wastes are found or it is discovered that Sigmon Septic Tank
Service has been operating a hazardous waste disposal facility, the
N.C. Hazardous Waste Section will assume jurisdiction of the
subject site.
We are currently holding the DEM August 9, 1990 NOV in
abeyance, pending the timely completion of the sampling required by
the Hazardou? Waste Section. If the sampling reveals that.
hazardous wastes are not present, the DEM Groundwater Section will
re-instate the NOV. We would then require that a complete site
assessment be performed to determine the extent of the soil and
groundwater contamination. You would also be responsible for
developing and implementing a plan to restore groundwater quality
based upon information gathered during the site assessment.
If you have any questions concerning this matter, please do
not hesitate to contact me.
cc:
Sincerely, r, ...
~-/J---~c~
Chris DeRoller
Hydrogeologist
,_r--·i1 '!._,,-~ .. , ... ,
. d t t ~ I. ·t• -si ·. ••j '-_; .: ;--1 •. Inci en Managemen Uni t -· •
-' Hazardous Waste Section, o 1., qq,1 Solid Waste Section
CMD/pl
Mr. Phillip E. Powell.
April 8, 1991
Page Two
Based upon the soil sampling results, this Office will
determine if additional site assessment, if a monitoring program
for your water supply well, or if some other type of action will be
required. You will be informed of this decision in a separate
letter.
Please submit the soil screening and laboratory results along
with a map showing the drum storage area, soil boring location and
your water supply well location within thirty (30) days of receipt
of this letter.
If you have any questions, please do not hesitate to contact
me.
Sincerely,
/) j ,,'\ ./'? .1;,' ;/// . .i/ 1,/ /,/,,:;:
(_/'f/V..,--:J / ._J',~t-1__,.(_-~,,..__
Chris DeRoller
Hydrogeologist
Attachments: DEM Sample Results
cc: · Incident Management un~t7
CMD/pl
REC£.\\/£D
~p?. \) 0 (i"i I
l'OLLIJ"\\O" co""\ROL sAA"C~
State of North Carolina
Department of Environment, Health, and Natural Resources
Mooresville Regional Office
James C. Martin, Covernor
William \Y/ Cobey, Jr., Secretary
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
Mr. Phillip E. Powell
Albert F. Hilton, Regional Manager
DIVISION OF ENVIRONMENTAL MANAGEMENT
April 8, 1991
Appalachian Chemical & Solvents, Inc.
Route 1, 333-A
Granite Falls, North Carolina 28630
Subject: Appalachian Chemical
GW Incident #6374
Alexander County, N.C.
Dear Mr. Powell:
The Mooresville Regional Office Groundwater Section received a
copy of the groundwater sample results from your water supply well
on April 1, 1991. Based upon these results and the Division of
Environmental Management (DEM) results from your well and two
neighboring supply wells, it would appear that the groundwater
beneath your facility has been impacted by a release of
tetracJ;i_loroethylene ( PCE).
Ci ·?\IJ:J~~,,., . _ In· the .. ,£egJ,ufry 18, 1991. Notice of Violation issued to you by
DEM, you were requested to inspect your drum storage area for signs .. \) . .. of spills or :J,.E(aks. Due to the nature of the soils at your
facility and the mobility of PCE in the soil, an adequate
i;s·p'e'tt-:i'.dri:J.wji:lli,require at least one soil boring to auger refusal
in the drum· stoi:/i!~'e area.
Soil samples should be collected at 5 foot intervals and
screened with a field meter. One soil sample from.the area with
the highest field meter reading and one soil sample taken near the
depth of auger refusal must be submitted to a laboratory and
analyzed using EPA Method 8240. Please report all parameters
included in the Method 8240 analysis whether or not a positive
identification was detected.
919 North M;iin Street, Mooresville, NC 28115 • Telephone [phone] • !:AX 704-663-6040
An r-n11:1I Onr..rt11nitv Affirm:itivr A,·tinn J:mnlnv,•r
.(
State of North Carolina
Department of Environment, Health, and Natural Resources
Mooresville Regional Office
James C. Martin, Covernor
William W. Cobey, Jr., Secretary
CERTIFIED MAIL
DIVISION OF
February 5;
RETURN RECEIPT REQUESTED l?tc .
Ff8 't111to Mr. Barry Sigmon
A.A.A. Enterprises,
Route 14, Box 350
Statesville, North
o·ear Mr. Sigmon:
Inc. Po1LIJ 6 /9·,, < Tt.o ,,, Carolina 28677 . fl' COi(
TRoL
RE: Request fo:r::_Extension ~RA!rc ,
SiglTl~']=Septic-Tank--Ser.v~e _
Groundwater Incident No. \:.3_422.J
CireaeD._.county, N.C.
As per our telephone conversation on January 30, 1991 your
request for in extension to submit the sample results for the two
newly installed monitor wells is granted until March 15, 1991.
The samples should be analyzed for metals (including mercury),
nitrates/nitrites, chloride., and organic compounds. The samples
for metals should be· filtered prior to analysis. EPA Methods 601,
602 and 625 must be used for the organics analysis.
This will be the final extension for the submittal of the
groundwater sampling res~lts. Failure to rispond within the time
specified and to voluntarily achieve compliance may result in the
recommendation of enforcement action, including the issuance of a
special order against you under the authority of General Statute
143-215.2; or a request to the Attorney General to institute an
action for injunctive relief.
919 Nonh Main Street, Moon:wilk:, NC 28115 • ·1t:lcrhom: 70-4-663-!699 • FAX [phone]
An Equal Opportur_1ity Affirmative Action Ernplnyer
Mr. Barry Sigmon
February 5, 1 991
Page Two
If you have any questions, please contact me at (704)
663-1699.
Chris DeRoller
Hydrogeologist
cc: Perry Nelson, Groundwater Section Chief
Keith Masters, Hazardous Waste Section
Lee Crosby, Superfund Section
Steven Clayton, Solid Waste Section
CMD/pl
MEMORANDUM TO:
THROUGH:
FROM:
RE:
DIVISION OF ENVIRONMENTAL MANAGEMENT
February 4,
Keith Masters
Barbara Christian l-c
Chris DeRoller C .u vJ
1 991
ts I gmon ... Sept:iTYank:~serv ice]
(A.A.A. Enterprises, Inc.)
Groundwater Incident No. [3"422]
il:reae·1·1-·county, N. C. --~
On June 14, 1990 I sampled two State monitor wells located at
the subject site. Elevated levels of metals, including mercury,
and 1,1-dichloroethane were detected. A Notice of Violation of 15A
NCAC 2L groundwater standards was issued to Sigmon Septic Tank
Service on August 9, 1990.
On August 29, 1990 I received a call from Karl Shafer of the
Solid Waste Section to arrange a meeting at the site to discuss the
closure of the lagoons. Karl Shafer, Steve Clayton, Scott Readling
and I met with Mr. Barry Sigmon on September 5, 1990.
During this meeting, it was decided that Mr. Sigmon would need
to determine if the waste in the lagoons was hazardous prior to
land applying it and filling in the lagoons. The Hazardous Waste
Section agreed to specify the type of sampling required for the
lagoon wastes and the Groundwater Section said that it would
require two wells to be installed and sampled near the lagoons.
The sampling results would then be used to determine what further
actions would be needed and who would be the lead agency.
Mr. Sigmon had the wells installed in November. He contacted
Scott Readling to determine what sampling would be required for the
lagoons. There was some confusion on Mr. Sigmon's part as to who
was responsible for sampling. Consequently, no sampling has
occurred to date.
I spoke with Mr. Sigmon on January 30, 1991 regrading the
groundwater sampling. The Groundwater Section is requir{ng that he
immediately sample the two new monitor wells as per the August 9,
1990 Notice of Violation. If groundwater is impacted, we will
require that the lagoons be closed and the extent of contamination
be determined as per 15A NCAC 2L .0106 unless the site falls under
the jurisdiction of the Solid Waste Section or the Hazardous Waste
Section.
RECEIVED
FEB 6 \9:ll
POLLUTION CONTROL BRANCH
Page Two
There are three drinking water supply wells immediately
downgradient of the lagoons and several-other wells in the area.
There is no nearby alternative source of drinking water .. Neighbors
in the area have also expressed concerns that the lagoons
.themselves represent a safety hazard as they are not securely
fenced off from the neighborhood.
Please advise as to who will be the lead agency for this site.
If the Groundwater Section is to be the lead agency, please provide
us with the sampling requirements necessary to determine if the
waste in the lagoons is hazardous.
cc: Perry Nelson, Groundwater Section
Bill Meyers, Division of Solid Waste Management
CMD/pl
(
N.C. DEPARTMENT OF NATURAL.•RESOURCES LAB NUMBER e
NO.
go' 5g ' 1?. '' ~fM l,LJ0 TODY I Roe a by: . , ,om· Dus·~
10; A~O. FRO, G-5 ARO, WaRO, WiAO,
E{}lf/ftNNlj')Yr-°~f~~PMENT G OAT.E RECE"/Js/-«~-9~
GROUNDWATER FIELD/LAG FORM · r~er-11------~-----=--c-
SAMPLE PRIORITY
Kinston FO 0 I her
Shi6pea by: Bus,
·coL.LECTORCs.J: --'-'+-""-'-'+CL __ DATE
-~ ,,
FIEl.'D. ANALYSES
·PH ◄ o·o --~-Spec. Cona.94 ___ at 2s0 c
Temp.10 ____ 0 c Oaor _______ _
Taste ______ _
f :aid Analysi_s By:----------~--
□
TIME
Owner
ROUTINE
10 5 '!O
~
fl lle r
Localion or si1e
d
G
Oescrip1ion of sampling point
Sampling Me!hoa
Remarks /),.l/ ,J,>/', ,,-, .,,//·p,;,+
-I-we ii
C {' <"",,, -.L.,; C ,o le. r ,a C
LABORATORY ANALYSES
(!.,., ,ec)
I . rs,·~ -I'")/)'$"
I v _ /'.--.:.:._-Ding !\':2j·-»\1emp, e1c ·• r Ue{f C nl,r ...,...c,,..lr '•'>/!.,.,// c...p -=? ¥ ::J:)
I .. ,-•-•-~,r·~;:.~~\\\\Jt /
8 OD~ ' ,0 m O /l Sol J Q, 7 r,)~ 00 mo/I " s,1v11 1 on .-\ :~· :; t_o/1~ t :1 \ 4 O101nocn10,,"• P • I !IC•~ t >
COD Htol'I ', 0 moll·
COD Lo ... :i"n mg/t
Fluo
Hud
Al r. -. I IC) 5 , ... -·---, .. ; --~} \\ Org,nopn01:::no,,.-1 ;> o I !1 CI~ O I de, '" ffiQ/1 "Jvminum IJQ/1~
n1u;To11I i0,0 moll ,, 81 !i~-~·.:, 00 7,; v.011 V
V Colllorm:M~ F101 J \ 6 l 6 ~1 1100ml Hire (non·cuo) c,1~i,,;,;,_916 ,,.-...t•
n, '' ,01 mo/I c, ., 1 '\_·:,~Q/J Atid )'hrdicieu
Coliloim:MF lo I~ I ) l ~ 0 ~ 1100ml
TOC '" m,;,/J
pr,.,
SPI c
101 J C ·• e~-1-urfl'• Io 2 7·,-'-:;_'C) .. -
i :in:io 1.10/1 Cd UQ/1 :\ i ( ~\
Ille Cone. " 1.1Mho·s/tm 1 C/\1omlum:Jo11J lOJ• .• ..,-'(Q ~I.~\ 81 U I Nt~lr II E • 11 •',.ti, 0 J QI !\It I
Tvrbldll7 " rnu Sul! "' '" m9/I c, COP Plf ... 1.0.,.~ \ \ \--\ D'-1~ f'. 1 :, ·, ,,i.C' AC i e f J t/ IC I, 0 I I 0<:; I•~• CI
.. S vii ". '" <noli ,. lr~n 10H1'-Q C-...\J:,.\\:t.ll1uo/l
--Ho Merci.rlr 11 sicio 1.1011 y Pv10,~1:11, Oqi,"i:1 ('~QA t, 0 Ill 1}
'" '" units K -Pouuium '" mg/I
... n.1lril17 10 pH•.~ ., 0 mg/I MO M1on11ium '" mo,, I• l OitHOmOt I"'"' ! 0:) 5 l
>,I~ iJ i nl ly " '" .. ' ., ' mo/I Mn• M1no1n•11 \OB VQ/1
Cubon1t• "' m9/l No Sodivm '" m9/I
Bli;u1,,on111 "' mg/I .. H • 5 1 0 mo/I NI NI c :-. ·,1 1015 7 I.IQ/J \ I Arunlc:To\11 1002 \JQ/1 TKH .. N 525 mg/I Pb Lnd 105 ! uo/1 ~ a...l.-l.-.. •-l'\~•&.IIJIII.$; NI 'IJ
Cirbon dlo.JJdt "' mQ/J "H03 ., H "' ITIQ/1 s, Stl1nium 110 uo/J aau,...-..-
Cl'IIOfld1 9 ◄0 m,;,/1 P: To '" " p '" mo/! Zo Zinc 1091 uo IJ.
. 'Cl'ltomfum:H11 I0J2 UQ JI
Colo1:T1u1 10 Pt·C o
Cyanide T 20 molt
.
Lab' Comm en Is::~-----------------------.,..-------------------'--~-------------------------------
GW·5-4 Revised 7185 for Dissolved Anal'fsis · sui.i:nil liltered samotc and write ·01s· in block
While copy ··Headquar!cr:; Pink copy· Region Yellow copy• Lab
<.)
VOLATILE ANALYTICAL PEPOPT
LAB NO. 1G102
REPORTED BY ~ ENTERED BY
CHECKED BY ~ CHECKED BY
REVIEWED Bl' ~-
SUPERVISOR :tiK DATE i/t/41
.S/\MPLE TYPE: WATER
ANAL Y31S RESULTS
STORET NO. COMPOUND
39180 TRICHLOROETHENE
34475 TETRACHLOROETHENE
DETECTED BY GC/ELCD.
NO VOLATILE ORGANIC COMPOUNDS DETECTED BY GC/PI D.
bd,
DS
CONCENTRATION
0.35 UG/L
0.29 UG/L
..... . ·-....
' ,
,
/ I
~tCt
trur lVtD
PolL11r,off 4 ,~~
State of North Carolina CONrfiol
Department of Environment, Health, and Natural Resources . . 81iAN,c/f
Mooresville Regional Office
James C. Martin, Governor
William W. Cobey, Jr., Secretary
Albert F. Hilton, Regional Manager
DIVISION OF ENVIRONMENTAL MANAGEMENT
November 7, 1990
Mr. Barry D. Sigmon
A.A.A. Enterprises, Inc.
Route 14, Box 350
Statesville, North Carolina 28677
Dear Mr. Sigmon:
RE: Request for Extension
Sigmon Septic Tank Service
Iredell County, N.C.
Your request for additional time for submitting the sample
results from the monitor wells and the pits at the subject site has
been reviewed by the Groundwater Section of the Mooresville Regional
Office ..
Based on the information you have provided to the Groundwater
Section with your request for an extension, the request is hereby
granted until January 15, 1991. You will need to contract someone to
collect the samples. You may want to contact Scott Readling with the
Hazardous Waste Section at [phone] to determine how many
samples to take and what to test for. I have also included a list of
consultants located in North Carolina.
Should you have further questions regarding this matter, please
call me at (704) 663~1699.
Enclosure
cc: Of,fice of Gene_ral Counsel
.;i'hcident Management Unit
CMD/pl
Sincerely, ~/~ Chris DeRoller
Hydrogeologist
919 North Main Street, Mooresville, N.C. 28115 • Telepliom: 704---663-1699 • FAX 704-(I03-6040
An Equal Opportunity Affirmative Action Employer
,;.:;. . 'l
J
State of North Carolina
Department of Environment, Health, and Natural Resources
Mooresville Regional Office
James C. Martin, Governor
William W. Cobey, Jr., Secretary
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
Albert F. Hilton, Regional Manager
DIVISION OF ENVIRONMENTAL MANAGEMENT
August 9, 1990
Mr. Henry Sigmon, Jr. Sigmon Septic Tank Service
Route 14, Box 350
Statesville, North Carolina 28677
Dear Mr. Sigmon:
RE: Notice of Violation
15A NCAC 2L Classifications and Water Quality Stand~rds Applicable to the Groundwaters
Sigmon Septic Tank
Incident No. 3422
Iredell County, N.C.
Chapter 143, North Carolina General Statutes, authorizes and directs the Environmental Management Commission of the Department of Environment, Health, and Natural Res·ources to protect and preserve the water and air resources of.the State. The Division of Environmental Management has the delegated authority to enforce adopted pollution control rules.
Based upon an inspection of your facilities located on Route 14, Box 350, Statesville, North Carolina, the Division has reason to believe that you are responsible for activities resulting in noncompliance with North Carolina law. Staff of the Mooresville Regional Office (MRO) of the Division sampled two monitor wells at the subject site on June 14, 1990 and the lab results indicated that the North Carolina groundwater standards have been exceeded.
Specific violations of 15A NCAC 2L .0103(d) -No person shall conduct or cause to be conducted any activity which causes the concentration of any substance to exceed that specified in 15A NCAC 2L .0202 -are as follows:
919 North Main Scn:.-et, Mooresville, N.C. 28115 • Telephone 704-()()3-1699 • FAX [phone]
An Equal Opportunity Affirmative Action Ernployer
\
Mr. Henry Sigmon
August 9, 1990
Page Two
Concentrations of Substances Found in Exceedance of 2L Standards on June 14, 1990 (in micrograms per liter, ug/1)
Constituent MW-3 MW-4 2L Standard
Iron 590 2300 300 Lead 86 190 50 Manganese 430 50 Mercury 6.0 <0.2 1 . 1 1 , 1 Dichloroethane 1 . 3 ND ND
(ND -not detectable; --means not analyzed for)
You are responsible for causing, contributing or allowing the continuing violation of the underground water quality standards because you are storing septic tank waste in unlined lagoons.
To achieve compliance with the above-cited laws or regulations, you are required to submit "within sixty (60). days from receipt of this letter a site assessment report as prescribed in the enclosed outline. As a part of the site assessment, two monitor wells should be installed in the vicinity of the state monitor wells that were accidentally damaged. This data will then be used to submit a remedial action plan which will be due'.within sixty (60) days after the site assessment report is submitted and approved by this Office.
The above violation of 15A NCAC 2L is subject to a civil penalty assessment under the authority of G.W. 143-215.6 of not more than $10,000.00. Failure to respond within the time specified and to voluntarily achieve compliance may result in a recommendation for enforcement, the issuance of a special order against you under the authority of G.W. 143-215.2, or a request to the Attorney General to institute an action for injunctive relief.
Your response and/or questions should be directed to Chris DeRoller of the Mooresville Regional Office at [phone].
cc: Office of General Counsel
I.J.>&ry Nelson
Sincerely,
Brenda J. Smith, P,G.
Regional Supervisor
Enclosures: Site Assessment Guidelines
,Sample Results
CMD/pl
cci",:,·r v L r"'"e...,_r,'"'-}e,....t ... 1/ _____ _ N.C.
OUAI) f/O.L67Ct'J SERIAL NO. Ile 'lt?t
DEPAf<-.,.,MENT OF NATURAL REsouRECEfVEBMBER a Clq. & IL:/ ~
& COMMUNITY DEVELOPMENT ~• DATE RECEIVE,/411/S/46 T,meqJ.::,
OEM 'LJL <'.'. , lcteic\.ld ~ From Bu~ LAT. 3,:0 '-(3'[)£" LONG. 5oo ,=g-'c,,;-I(
Report to: ARO. FR~. RAO. WaRO. WiRO,
GROUNDWATER FIELD/LAB FORM Qthl\h--,,...;,.,--~-------~ .
rvllUTIO NTRvL o~ANCA · <Ji ----:----'--..5
~t1Aj-EftiBl~fi~T(\l'\y DATA ENTRY BY:-=o CK·'-----' WSRO, Kinston FO Other _______ _
Shipped by: Bus,~. Other
COLLECTOR(S): r/,Jf;1244(;r
rim1"1c VO l.!rlJ~if"'-"lJ DATE REPORTED: 1-A'-i:80
DATE -ti -3 't;i 2 t5/l'f/zlJ TIME , PURPOSE: BASELINE, COMPLAINT, COMPLIANCE, r.us·. -~
(circle one)
FIELD ANALYSES Owner ~,,, le Sc-r r/2'ce
pH 400 ____ Spec. Cond. 94 ___ at 2s0 c Location or site ,c?:fC-tl I±
Temp. 10 ____ 0 c Odor NO'Y1J? Description of sampling point We&!~
,{)U,dJ ( Taste ~,v=--.-/.~4f.,__
Fie Id Ana I y s i s 8 Y: ___ ,__Q~_,f~@=,,_/;~ffc.~~---
Appearance
Remarks
Samplin~ Method ~ (pump, bailer, e1c·.)
,,.--, ,,:-I Sample I nterva I ---L"----'IL'---------
(pumping time, air temp, etc.)
LABORATORY ANALYSES
BOP5 310 mg/I Olss. Solids 70300 moll V Ao • Sit~,r 1077 ;; r, " . ug/1 Organochlor!ne P•stlcid••
COO High J◄O mo/I Ftuorlde 951 moll Al • .,1umlnum 1105 '?,ciOO ug/1 Organopnoaphorus P•1llcide1
COO Low 335 motr Ha.rdness:To1a1 900 mo/I V' •• -Barium 1007 7' i"I uc;i/1
Colilorm:MF Fecal 31616 1100ml Harctn•ss {non-carb) 902 mg/I c, -Calcium 916 mg/I Acid Hardicid••
X Colil1.,rm:MF 1otal 3150◄ < ll"-l11oom1 V Phenols 327JOA_J<-i ug/1 y Cd • Cadmium 1027 ,:_7 l't ug/1
TOC fi80 mg/I Specific Cond. 95 uMnos/cm 1 v Chromlum;Tolll 103◄ L7C: uc;i/1 l.x Be•• / Neutral Extrec1.1bl• Organic1
Turbictily 76 tHU Sulfate 9◄ 5 mg/I Cu -Copper 10◄2 uo/1 X Acid Ex1rac1lbl• Organic,
Sulflde 7 ◄5 mg/I Ix-Fe -Iron 10◄5 l.'lQC, ug/1
\,/ Hg -Mercurr 71900 ,:,r,.7 ug/1 IX Purg•able Or~i,i:~~p~:..__~ttl•)
pH ◄OJ uni 1s
Alkaflnily topH ◄ .5 ◄10 mc;i/1
Alkalinlly 10 pH 8.3 ◄ I 5 mg/I
Carbons ta . " mg/l
K • Pocassium 937 7. ··-mg/l1f,"'
, __ -~'·"'w,1u \1 .. ,:1r• ~..., ,, 1G \.. \ 1 ;{
M11 -Ma.gneSiulll 927 I, I~ mGJ• Jl \ ~-: .. ~jt· . .:Oib;~m10~1hl£1~ ~9:S,Jt
Mn • Mam;1.1nesa 1 Os s L. ."'{) ug/1 '1, ) .:,.., ·•·; ·l;J
N~ -Sodium 929 s.4 moll -, i\ ,, ~~ ,ac,n .. "
Blcan.onate HO mg/I NH3 "N 610 moll loO JUt. {..1~/ --· Ni -Ni ck el 1067 ug/1
✓ Arsenic:Total 1002 L, {() """ TKN u N 625 mgtl V PO -Lt ad 1051 I'iO u11/I --~ 0cF>T\f\N . mg/I Carbon ctloxlcte ◄05 N02-,. N03 as N 630 moll s, Salenium 1 1 ◄ 7 <e5_7\ uo /I GI O\J j~LJY'{r\l l.i\ u,'":~ ., .. .:r•r
Chlorlcte 9 ◄0 mg/I P:To1at as P 665 mg/I '\ lo Zinc 1091 "'(rt ug/1-' nY I\ '\Ji. r \'.i t1 ~ '-I"'' -,
Chromium:Hex 1032 ug/1 _l.,l~ALl::>1;:) tH-
Color:True 80 Pt-Co
Cyanld• 720 mc;i/1
Lab Comments:
For Dissolved Analysis -sui...mit lillered sample and write ·01s· in block
White copy -Headquarters f)ink copy -Region Yellow copy -Lab
LAB NO.
REPORTED BY
CHECKED BY
REVIEWED BY
SUPERVISOR
SAMPLE TYPE:
STORET NO.
SEMIVOLATI LE ORGANIC REPORT
OG610
MD /rzJ ENTERED BY
~ CHECKED BY
~
'17eK DATE t,p~/q i)
WATER
AHAL YSIS RES UL TS
COMPOUND
NO BASE/NEUTRAL OR ACID EXTRACTABLE ORGANJCS DETECTED
BYGC/MS.
\ ' '
ill os
(
CONCENTRATION
(
VOLATILE ANALYTICAL REPORT \,
•
LAB NO. OG610
REPORTED BY r'~ ENTERED BY 00
CHECKED BY (//I!, CHECKED BY Os
REVIEWED BY ~ MTE1+-SUPERVISOR ,teK
SAMPLE TYPE: WATER
ANALYSIS RESULTS
STORET NO. COMPOUND CONCENTRATION (
NO VOLATILE ORGANIC COMPOUNDS DETECTED BY GC/ELCD/PI D.
(
(lJI.:•! rY
OUAll no_L{,, ?Ct '6 SERIAL w). TR'i{.'7.(
ro g: OR LAT. _;5~S::,__~'f_3,__0_]~ LONG.
N.C. DEPA, ,v\ENT OF NATURAL RESOURCES
& COMMUNITY DEVELOPMENT
LAB NUMBER 8 ~ {p/ I
DATE AECEIVE0"2/21.J17'<'.'.:J Time C);,S-
l'UA DEM Rec'd b~ From:
Repor! to: ARO, Fno.§ RRO, \'/aRO, WiRO,
GR O~IN-R(l[!-D j.,L AB FORM
s A M p L E flp, I CW, lfS T O'f) 0
OAT A ENTRY BY:
0 the r ------=--------,--c---,~-
j),9 CKl~ D WSP.0. Ki11s1on FO
Shipped by: Bus,
FIELD ANALYSES
Other
DATE
Owner
□ ROUTINE O El.1EAGENC y DATE REPORT E O: __ J.c.'~-,....,36...,_-_q_..,( __ ,__ __ _
TII.J E i :_5 0
____ Soec. Cond.94 ___ ai 2s0c Location or site
Tern o 1 0 ____ ° C Odor ---~4_,c_' ~O~CLJ2-.= :EEC,ElYT:ID poinl/:S.~c,~/_-,_l~cC.;,.-.,r::,__ _______ S I I '-""' :::C:,c:;/ •,A,i• ,\n:1earance fil,,Jrlv l
LABORATORY ANALYSES
BOO~ :l I(}
COD '11 Ql1 3'0
co•":, L ,>" '"
Culrlorri;Mi I ecal J I 1J 1 r,
mQ/1
rn,:i /I
mQ /l
/ 1 OOMI
y Col1!,.1m:'.1f Tola I J 1 ~o • L. In, 100ml
iOC: ,:a o mQ/1
T ur:i, ,1, Ty 7 6 :nu
'" 4(),:0 uni ts
Al• al I n11y 10 l)H .., ., 0 <ng/1
Al' alin,?y ,o '" ,. J ., , mg/I
Carconate ... s mo/I
9,car, .Jna te • '° mg /I
X A.1se,,ic.:T01al l 00 2 ,: I 11 ug/1
,;art>on <1,0,.de ,o, mg /I
(.,nlo"Ue 9-'0 mg/I
CMor1>u<"l:He• 1032 UQ/1
Color:Tru~ 80 P1-Co
Cyani.:l" '20 mg/I -
\'
1 \(lC,)Q (pumo, t,aiier. etc~ amp e nte_\'i/iQL,"1{i)w,4 j. , , , ,.
Hen1af,fjG __ ]._ f.i+.+ · ·• '--vf1url
(pumping _time, air tfu filti.i/ii, NC
"n111\TiON J ~ L t
Orss. Solids 70300 mg/I /< Ag Siher 1077 C: ."\"' II ug/1 Org,nochlorine Pesticides
Fluoride 95 1 mg/I " .\luminum 1 ! 05 I "l(10 UQ/1 Oroanoonosot1orus Pest,cid•s
Hardne~s:Toial 900 mg/I X ,, Barium 1007 79.() ug/1
,_,a1dness (non-carb) 902 moll c, Calcium 916 mg/I Acid HerdiCtdeS
Phenols 32730 ,\\ <, ug/1 A Cd Cadm,um 1 0 2 7 L.Z,C) ug/1
Soecitic Cond. " uMnos/cm7 y Chromium:Total 1 OJ" "-2.5' ui;i /1 v 811 SIi I Neu I re I E,1ractao1, Oroanics
Sulfate 945 mg/I Cu -Coooer 10•2 uo /I ,)( Acid Er tractable Oro•n1cs
Sul! i Cle ,. , mg/I ,'<.. Fe -Iron TO 4 5 o:.qa UQ/1
:-<' Hg 1.1e1cu1y 7 1900 I. J') uo/1 X Puroe1bla O,o,nics {VOA bottt el
' 0otassium 937 mg/I
Mg -Magnesium 927 mg;< '' z ~ 01bromoe1nan, {EOB)
Mn -1.1anoanese 1055 UQ/1
ra Sodium ·929 l':l mo/I
,'lH;j " N 610 moll Ni r~ IC k el 1067 C I ug/1
Tm as N 625 mg// X " L II aCI 1051 rn -uc/1
NQ2-tN03asN 6JO mg/l s, Selenium I H7 ug II .......... :'' .. ,....,, l(.l,I UKL1At·J1CS
-·
P:Total as P 665 mo/I ,x. '" 7. inc 1091 43 uo /I • "., ,._ 1 :::i1~ KU--'UHT
r·or Dissolved Analysi~ -sut,-riit fi!lcred sample and wdle ·01s· in block
V,'hitc C'J(:y -licall1nJarter:: hr;;. r,r.,1:y -Re,iion Yellow copy -Lab
VOLATIL£ ANALYTICAL llEPOllT
LAB NO. 0(;611
REPORTED BY
CHECKED BY
ENTERED BY --1.ffi...,_._ __
REVIEWED BY !l/&
suPERVISOR rJ:,eK DATEffe
SAMPLE TYPE: WATER
ANAL VSIS RESULTS
STORET flO. COMPOUND
34496 1 , 1 DICHLOROETHANE
39180 TRICHLOROETHENE
ONE UNI DENTI Fl ED PEAK DETECTED BY GC/ELCD.
ONE UNIDENTIFIED PEAK DETECTED BY GC/PID.
CHECKED BY
THESE COMPOUNDS WERE TENTATIVELY IDENTIFIED.
~
CONCENTRATION
1.3 UG/L
0.18UG/L
LAB NO.
REPORTED BY
CHECKED BY
REVIEWED BY
SUPERVISOR
SAMPLE TYPE:
STORET NO.
,·
SEMIVOLATI LE ORGANIC REPORT
OG611
MD/tz; ENTERED BY rf)
~ CHECKED BY D5
~
rJ<.it::.. • DATE~
WATER
ANALYSIS RES UL TS
COMPOUND
NO BASE/NEUTRAL OR ACID EXTRACTABLE ORGANICS DETECTED
BYGC/MS.
· CONCENTRATION
. '
COU/HY
OUAO t·JO/_.(,, 7/). Ji
LAT. J~ 'f3
SERI AL NQ_r./li? lf(;,JS'
0 'l-L Of✓G. ~/?<? __ .s:r~_tJ_f~
I, I,
N,C.J~_,PARTMENT OF NATURAf'\lj'JA
i & COMMUNITY IJEVELOP~f'I I f) E,\,\
Report lo: ARO, FRO~ RAO, WaRO, WIRO,
\/✓SRO, Kinston FO 0 ther
!GROUNDWATER FIELD/LAB FORM
_S_A_M_P_L_E _P_R_I O~R~I T_Y_ .Jf "t} ')--
ROUTINE ~v1ERGEf✓CY ~
Othe, ~,)
DATA EIHRY BY~~ C:K:~
DATE REPORTED: /I -3 c., -,f 7
Shipped by: Bus,a Othe,
COLLECTOR(S): -~~~~==~--DATE
FIELD ANALYSES
pll 400 ____ Spec. Cond.94 __ at 2s0c
Temp.10 //, 0 c Odor /Jon<'-c
Owner
Loca ti
D
Tl i.lE 15"/t;
S:,2J .,....,,5
n a, site SI!'
PURPOSE: BASELINE, COl-.iPLAIMT, COi,1PLIAMCE, LUST,
{circle one)
S' ,f:t· r • I "a k $" «"'V-·, c;. <
1,33 .,vt,w, --3
Appearnnce Jn,..Jj Y ;ast'i N hj
Field Analysis By:{, fM ,
Oescri.wian ol sampling .pain! ,c.. ""'.Z ~ ✓
Samp11JC1 f·,1e1hod _J(3.",~C.~-~/L_,~J~"-,-----------------Sample Interval-~-'~.;,~-----------!, -,--. -~~ump, baile,, etc·.)
(pumping lime, air temp, etc.)
Rema<ks . .L-nc J.,.,;;t -'%t: Yt2z
LABORATORY ANALYSES
BOD5 310 mg/I Diss. Solids 0300 mg/I ' Ag -Silver 1077 ug/1 o,ganochlorine Pesticides
COO High 340 mg/I Fluoride 951j mg/I " -Aluminum 1105 ug/1 Organophosphorus Pesticides
COO low 335 mg/I Hardness:Totaf 900 mg/I •• -Barium 1007 uo/1
Coli1orm:Mf Ft:ocal 3 lti 16 1100ml Hardness (no\1-carb) 902 mg/I Ca -Calcium 916 mi.II Acid Herd1cides
Coli!orm:Mf T 01at 3 1504 1100ml Phenols 327~0 uo/1 co Cadmium 1 0 2 7 U\j/1
TOC 680 mg/! Speci1ic Con~. 05 uMhos/cm1 Chromium:Total 1034 ug/1 Base / Neu1ral E•traclable Organic,
Turbidity " rnu Sulfate 94CJ ' I mg/I Cu -Copper 1042 U\l/1 Acid Extractable Organics
Sul1ide 745 i mg/I Fe -Iron 1045 ug/1
j Hg -Mercury 71900 ug/1 y Purgeable Organics (VOA bottle) I:>!< >-
pH 403 uni ts j K -Potassium 937 mi.JI /
Alkalinity topH4.5410 mg/I ! Mg -l~agilesium 927 mo1' 1,..2 •. -Dibromoe!hane (EDS)
Alkalinity to DH 8. 3 4 15 mg/I ! Mn -Manganese 1055 ug/1 "
Carbonate 445 mg/I I Na Sodium 929 mg/I
Bicarbonate HO mg/I Nl13 db N 61p mg/I N> Nicl<el 1067 U\j/1
' PO Lead 1 05 1 ug/1 ..
Arsenic:Total 1002 ug/1 l KN as N 621 mg/I
mg/I N02 • N03 a~ N s, -Selenium 1 14 7 ug/1 ·r:· '. Carbon dioxide at05 630 mg/I .
Chloride 940 mg/I P:Total as P ~65 mg/l Zo -Zinc 1092 ug/1
Ch1omium:H1:n 1032 ui./1 I '<
"' Color:True 80 Pt-Co "· .
Cyanide 720 mg/I i "•
~ ~ /',~ ~:,., .I;:~ -! ( d,, A '']?:. _ _/ f, -C(J /Lh OJJ Lab Comments: fi / >, )iv! _, --7 ,,::--, -r ...:2 /, ~--~ 'L: 27 ,,,d, /)_ -Jn £1. -r;;-./) J,, ,1 G (!/ / /JI D I I , .
I V . -/I /
GW-54 Revised 7 /85 F o, Dissolved ('nal ysi s -submit tillered sample and write(iOls· in block
While copy -radqua,te,s Pink copy -Region Yellow copy -Lab
• J~~-_.;...-cour i r 'i
ou,,,j·uo 1=J..J[LJ_'j_ ,;un;,L 110-:IR 4 ~ 7{,
lid 35 i3 oG ,01,,c 1£0 sf 05
FIELD ANALYSES
oti 400 57) 7spec. Cond.g4 .f:zX. at
TemD.10 15 °c Ooor Noa:s;..
,\ppeacance eJ.-.. Jd~~ T as,e f.·/A
t"ield Anal/'51S Sy: / ~J.. ; ;
LABO RA TORY ANALYSES
BODs J ,0 m11/I
COD hi Ch ,, 0 mg/I
COD LO• J J5 m-.n
Colitorm:Mr F t-C.il 3 16 I G / lQOmt
-Culitorrn:Mr Tot.ii 3 I ~O~ / lOOmf
IOC ~ ~ c, m11/I
T urt>i o It)' " rnu
"" ,o, uni I~
Al~dl lnl 11 " oh '.S 4 I(.) rn<;;/1
A I~ d Ii r1i If '" i,)'1 "· 3 "s m<;;/1
Cart>ondl~ "5 m<,1/I
Bicort>onat~ ~ 4 l'. m,; /I
>< Ars11nic:To1a1 l 00:> -c: ,'l ,-, u,;/1
Ca1t>on OIC•hlo/ ~u:. rn<,l/1
x' Cl"lloria., 9,o -~ mv/1
Ctiro1niurn:li.;• 1 OJ:' U'. /I
Coloi:Truot ,0 P1-Co
c,aniaw "" lll'J/1
Lab Cornrnents·
)/
)c
"
PURPOSE: GASE!....l!!E, COl.1flLAIUT, COi.1PLIAUC::, LUST. ~e;IJ; (circle une)
Qwnec S,'s Me,1S Sf:b-c :J:C,., !< $ 1:.<'.V•'< <,
L oc a Ii on o: s; le _(i.LfrL-_LI IL3L...J,_ _______ _,M'.ll.i./6,_),_.:_#.=-_,_lf ______________ ----'
Description 01 surnpling point ld ,_!/
Sa rn p Ii nq I.le !h Od _/3/;l,.JCJl~·~.Ji~~,;..,:JL __________________ Sa r:1\)1 e In !en a I _::3_;;2...-S:2..._1 _ _:: ________ _ :r , 1 (_~mp,, ba ;tel;, e!~-l Flemarks _ nc de tl .-,:i;t. ..). '-f 2..-'2..
(µurnping time. Dir ien10, etc.)
Di ~s. Sol j d s 10300 mg/I )(
r I uori cte 9S' me/I ;(
H .irdness: Total 900 mQ/1 ><
Hildnes5 {non·ca,ti) 90_2 rn,;i/1 I<'
Prieno~ J21l'fi -5 u,;i/1 X
Soec/!jc Cond. 9S uMl"lostcm 7 K
Sul!at11 9 4 t, 5( m,;i/1 X
Sul I ,oe I 4 ~ m ,;ill .)(
>('
><
I("
.x
>(
~;H3 " N b 1 0 , 0~ mg/I :X
1, . .-, " N t3 :>:, rn,;i/1 ~
t:O2 " t;O3 a, N 630 , () 7 mg/I "
P: T Old I " ' 66t. mull
,, -Sol• Bl 1071 ..c.:7.5 ug/1 J( o,,;anocl"lfor1n, P11o11c1ati
A> Alvminum 110'.i/.,.;;; ,,,,o v<;;/1
a, ea,ivm 1 00 7 ,iJ, lao IJQ//
Ca C.ilciurn 9 1 6 ,;;,q m<,1/I
c, Cadmlvm 1 027 < 10 -~c11
Cnrom,,.~:To101 IO 3 • 7,=:; :.;g/1
C-.: -Cooou 1 (}4 2 :Zc:J ere/I
" Iron l 0~ S J./E, 1:oD uc,/1
"' 1,1" f(;Ctf)' I l 900
, /') _.-, cr,;/1
' Poussium "' n me/I
M; /,tdQnt,;,um 921 ::) mo;,
/.tr. • •.1ancanese 1os5~Y1 oO u9/I
r;a Sor:, :;rn 9~9 .>f,·-r:,,.-1~~11
rJi /Ji C • t' I 1 o;; I ,, L '° JO.: ; CS I
s. S" I,; ni :;rr, 1 I ~ ?
'" Z Inc 10~:,;
" "
< ,=;[).'
/ 7 {j
<'70
i 70
,.
. ;_,,;ii.-' ?::{,",'.;~, .. ~ti
'-~/I
--\ao/1
'
:, .
i /.-:~/} ,.., ,..-n nRGAi"-1\.,""
··~ r:::::'\ .. ~ ~~-~r:-"Jt~~~
i \ ·,. i ---~ : 7 1 1
GW-:>4 Revised 7/85 f"or Uissolved Analysis· submit filtered sample and wrilu ·01s· in bloci-.. V/hile copy -Headqu.:irler:; Pi~h cop,,. -Region Yellow copy • Lab
I
Reported by (¾,?
Checked by ft1_.C_.
Supervisor~K
Lab No. Sample Type :
ORGANIC ANALY,IS
Entered by ),~
Checked by;OJn
Analytical Results
Date 61.//(el (o l I
Concentrati.on
' Q /
_,.., ·,~ ''"~·,,-On,.,,,·t111:n
f"rlr•--"'·"l.....(.I) ..
\) ' V
------+---------------------------t-------1
·-·-----+--------------------------+------7
·,
'
GC/MS/DS used
!'i---------;___..:....__ ____ ---'---_______ _
co1'lii~ _:r=~"~<--=¢~,-~l~I _______ _
& COMMUNITY DEvEt€}HA\N Uf: Ji:;A,"WE~E1vrnq-J7✓'{J '""• _9~10..,
N.C.'<::J":PART,\\ENT OF NATURAL RESOUR ~C!Q'f-"il/ER C =tC-:r 13 0 I
ou..;•.:: uo L_/,,,_'/{;-l(oc[RIAL fJO
>t"l (.) --i LC) " G . gv UEM / 'o by DaJ From Gu:<e)
f-, eµOI 1 IV
CROUNUIVATER FIELD/LAB I ORM 01t,cr
,.;f\0, rr,u.@"o) FlRO, '/✓aRO, \'/iFlO.
SAMPLE
'.'ISFiO. Kinstor1 ;·o 0 the:r □ ROUTIUE
G>'?o er •}_cl,, ,· .... ,-o 0 ,;_ T E. -"c...c f-'-_,1_-_L1... 1 I LIE , ;,
FIELD ANALYSES Owner S <Cr
Pi1.:;uo S~3'fspec. Conu.94:s,0 ~t 2s0c Loc:11ion or site • Stf I t 3 '!> /11,...J, 4 I
T emo. 1 o / 7 °c Oaor /10,CJ V
Appec1rance o:zeL/y Taste ,,-,,./ /n
Fir;ld Anal;·s1s By: L~
LABORATORY _.;t'-lALYSES
60(:..~ '.i 1 C, r.i';/1
(:Qt) hi<)n J 4 U m-.11
COLJ '" -JJ ~ mg/I
Coli lorm:Mf f t-CJI JI t, I G / I OOrr1 I
Colitvrm:l.li T r;:.,J :, 1 ~o~ / 100ml
TOC o e o mg/I
T uroi ui 11 " r:Tu
pH '°' l.lnl IS
Al ~a Ii ni I) ,, pH '-' 4 1 0 mg/I
A I~ al i nil) '" '" ,. 3 "s ffiQ/1
Ca,oundJ,:, 4 4 '., mo11
bica1oon«1,, "' mg /I
)( Ars11nic:Total 1 (JI,) 2 <//) U\j/1
Caroon 0,0,10'-' '" m-.11
X: Cnlori'j~ "' y mg/I
Cnromj•.,m:H~ • JO:);> U\j/1
Co1or:Trut1 " P1-Co
C y«n1,Jr no mg/I
Lab Comrnenls:
GW-54 Revised 7/85
Oescrio1ion ol sampling point
Sa mp! i na i.le th oa --~f1,,..,~i~:~/~<-d~-----------------S .J rnpl e Inter v 3 1 ....,-·J (pump, bailer, ~tc'.)
Remarks ~n c,.,~ !1J: # 3t 2 7,
(pumping tirnc, air 1emp, ,)le.)
OiH. Sclios 70300 m,i/l
Fl1.1oriOa 95 l mg/I
Hardna~~:Toldl 900 rng/1
Hd1dnass (non·cc1rb) '°' mQ/1
)( Phenols J 27 30 4 uQ/1
so~citic Cono. OS uMllOS/cm1
x Sulla111 94:, II mg/1
Sul I ioa 7' S mQII
.
Nfi3 "" N 6 10 mQ/1
Tr:N ,l $ /,/ 625 r moll
x N02 1' IJ03 ilS N 630 ,::; f.J-mg/I
P:To1al ~s P 665 mo/I
" "lumrnum 1 1 05 j /JI) Q◊Q UQII
X e, 6c1rium 1007 I r 0 (.) uc/1
c, Calt,um 91G er, m -.11
X Co Caom,um 10<'7 < /0 U<;:/1
cnromium:Toul 1034 -',-'5 UQ /I
x. C ·, Co oo~r 1042 -5';;:l ~ell
'' Iron I 04 5 ii'/ nob"•"
X HQ 1.1 ~ re ur) 11900W u,; /I
' Po1assium 9JT
"' Ma11n~a,um 9:.>7
V Sil s.,:~n,um 1 \47
._/ 7n i'tnc 109:'
,
dJ../-mQ/1
'-<' ?l' mo,,
:.C'] ','i' w;ii;-; ao 1.,) 'ug·,_•) (
For Oissolved Analysi!:i -subrnit filterod sample and wri!e ·01s· in blocJ..
White copy -Headquarter:,; Pink copy -Region Yellow copy -Liib
~ ~ ;r:-i_;✓-~, ~ ~-~~
1\~\~?tl ¼~\n
0fQ4~0C.ri"10;,,..'peHi~ice1' \
Reported by Cv,,
Checked by 6J..C.....
ORGANIC ANPSIS
Entered by~ Supervieo~
Checked by~
Lab No. Sample Type : I G --f;;, Analvtical Results
1G--\?,n\ 1'\, lA O.reJ;. l 0
r I ·_Q It" 01 o ~o , fQ _, 0, ', G C / f::\C'I,, -
'nc-,-• ..,,__, r (-Q O o M JA , ·))n. _-t,. .1, ·, ,I
""" 0
I l"' , ·~ n ,,i;-i Q .in _I) ,rn~ In r-On (¾ ; (1-o ...t 0 \ • A r:_r /e=-< -' V
Th~ '1 rM. n ➔ , £ o ~ _, -... ; " ,~n~ Or TTl ..J Q \ l A
-er V
\-' '""' Q ~ /le-Tin ,
rn~ .0 JU_..,, 0 fun , 4n • 0 ,n ~ r ;_Q O!Yfr, ~ rlr. 0,J)Q
(~\J'.J~ -· ' ,,. /) Aotn ,-fo ., 0)-v, (CJ / AA~ , V
'Y'ur n r,. ,Q J.,nnl~ _; Jon ,--.b-0 n ,-1-n ,o Qµ_, (: c__/ .:-, (_
V
..
.
I '-r-· ,-. . . -~_,-r·--,,·•·"t> ··1.r -; ...
~-··· ! · ' ' :-··' .. i 'f
'
I ' ... , --.. . -.• ·:irw
' " ,.,. ,,,-,
L., ·" . ·--'-" j • ,.,; I'(
' '' 1'' . 1-·! r:r~
.. ··--· -· . . ··-
GC/MS/DS used
Concentration
,, •
County:
Region:
Well Depth Screen Water Quad v.l lnter,al Samples No. I',.. To Lob ·,
I/,.. 7A/(,,(,' ?.4,0 W.·=,L/
{I 11/1 ::u1 , () · ?<'.1-34
18fi ,4, () 2-4-34-
'" r~' :"211. D . 29-39'
I lJ I
INCIDENT RESPONSE DRILLING SUMMARY
Incident Name: S~:S S!:f'ltt \i,;N~ Incident Number:_~scc4..__"2.=2.~------
Water-Soff Analyses Wells Geo-Wen
Date: __ 9_,_----'--B_-_8__,"l_--.---,---
Date(s) Drilled: 8·2 l/-8 7 't; e-25""-8 I
Geo-GW-1 Polution Remarks
table Samples In Surveyed phy,lcol Abandon logic Reports Confirmed B.L.S. To Lob File Logs Logs -----Tvne Z6,0? /es Yes Yes v.).[ ,h.._k_e.._ t-9'.72 ll ,, '' /f) .-.o. B ~2.b~ ,, ' ' ,, 33./ 2
{\ l \ ''
'
' ,; ,.'·
~i©!11\rt~ a~ SEP 2 19B1
INCIDENT DRILLING COST SUMMARY GROUNDWATER SECTION
RI\L£.\G\-\, NC
INCIDENT NAME'--'--'--'--'.:c.L"-"'-""''-"--"'S"{?'"P_7i,.,,cs.,.~• _,7i,:'J'l,,_N!«I-<::,_ _____ DATE BEGAN R·'tt.fl7 DATE COMPLETE $11-~,--H 7
INCIDENT # COUNTY ii?e'21?t1-QUAD # 1.·G?,-c,.
Cost--Personnel, NO. OF COST PER Material. Equip, 11R nn .. n M;lac 1'nnn Jnint~ ,rn n,,v I Mi 1 p Rqo l,Jni_nt 'TYYT'AT
Driller :rJ ,, " ;2</9.9?
In State Travel /t!J."'"',.C>b
Heloer :1-? 7, </J J_ / 3,5?
In State Travel /av.oo
Rio# ).J 2 l#'x ' /t:J,.,D ,!,0 J. 7,:;,oo
Service Truck ?/.fh •.1?l l'l; ,,:JO
PioeTruck
Loooer I 'j• .r ., 7c, . ·.'., '7,:,,""'
Loooer Van I ~Sh ':J'~-l"IJ/ -~o
Air Como.
Generator 15KW
Generator ·.5KW
Steam Jennv _;),_ J /;no-h"',Po /,-.t:,.:;) /() ;i...,oo
Sub. Pumn 7.5 HP
Sub. Pumo 3 HP
Pumn Truck . Sand 'll 1.:1. 00 J/,c;JO
Bentonite 3/8" 31 lq,"ftl 791,"0
Cement
Utilitv Trailer
Other
Pine
PVC SST. Steel Ft.
21'
X 10' 9 /J.,co J..-,<2,aa 5'
3'
2'
Screen Size
}( 10' # J...tn:70 /01,.1,00 5'
3'
2'
Surficial Protecting Cao
Above Ground Protecting Can ==r:x I I ,-J (,o,oo 1 //(!)1 oo
'. '~~q
GROUl'IDWATE.R JS,\ffilifON DRILLING COST
INCIDENT NAME ff/14). C ,M}!h}&):},,.e;~C_ 7'&u T>nAAJ DATE BF.GAN 8-.2~ -S'?DATE COMPLE'fE'?•,¾ £:;,
INCIDENT U · _ _,,J.J"'-"'~-c...· .,,__7-+--------------COUNTY ZU PE,U--_ QUAD # t -~ R-o· · . '
SUMMARY
Cost-Personnel, NO. OF COST PER Material. F.nuio. ..... .,., .. _ u;, .,.,.,.. u---1 ... .: _ ....... UD n... •. -M"'lo R.,n 1~, n• "
: Driller -,, /I SY",..,J-::, . '·~
Iri State Tra ~el -;i,:. ,oa .
,H<!l-nni;'., , < 7" ,'~o ... -i,
• •",[ •.• • •_c•• • • ·.·, .·. ;z,:,,,,,,, In State·Travel '.
-Rie' b • L. C: 1/~ It:, I.--,IJj) <o ~...-:-o ... " Service Truck /0 . .;-I!) -<,,oc
PineTruck
Lonner .. _.
Loooer Van
Air Cornn.
Generator 1511J
Generator 151-W
Steam Jennv 1 Y;,. . -o ,.._ . )Jl,--
Sub. Pumo 7.5 HP
Sub. Pumo 3 HP
Pumn Truck
Sand
Bentonite 3/8"
Cement 9 ,1./.v~-,,.,. ,..,...
Utilitv Trailer
Other ---II: ~LI,-
Pi.ne I
PVC SST. Steel Ft.
21'
10'
5'
3'
2'
Screen Size
10'
5'
3'
2'
Surficial Protectino Cap
I
Above Ground ProtectinQ Cao
I I
I' I~
Nct"th Caroli.nu
Department of Nlltural Resource.s and C-:-:r.:-;;· ... :~i~:y De\t·elo;;oent
Di.vision of Environ:-.1er .. tnl .M.c1nci~mt!nt
WELL ABANIXl.'iMENT
RECORD
P. O. Bo::c 'Zlt:Z7 -Rs.lei.;h, N. C. 2?611
1 •
REG. NO. ;;:==;;=;";====~ -= -•• •--•---•-••'-•"••M :J:.-;:.;c_-~j .. ~ rJ +--t=\:
WELL UX::ATION: (Shew a sketch of the location on back of form.) 3 1~:;
Nearest Town:_T..__._r_.o.,u"'+ ....... ro ...... e"""'----------county +£2-uD e I I
-~tJ...,(__"""'"',t;"-'-/ , ____ "'"S,...(£._-=-1_31 ... F__,,_,.----,,--,--,-....---Q;uadrangle No. /_ -b & ~:,
(Road, Comnunity, Subdivision, Lot No.) S.,ll,AL I± Ifl. '-157'1
2. OWNER: V&v,J C.t,u i;,,,.v,I'-..
3.
4.
5.
6.
ADmESS: ,Re <1:l-mee!
TOPOGRAPHY:draw,slope,hilltop,valle~
USE OF WELL: 7g [!)!' o ~.s DATE: ?,-,2(;-g-7
TOTAL DEPTH: zr ~ 5'L/ DillMEI'ER: .;2..
7. CASING REMJVED:
feet diameter
,2''
8. SEALING MATERIAL:
9.
Neat cement
bags of cement.J...:i"
gals. of water-9._
Other
Sand cement
bags of cement
yds. of sand
gals. of water
Type material ____________ ,
Amount ------------'-------EXP Lfffii METHOD OF ENPLA.CEMENT OF MATERIAL
' Cfmeui mueJ
I do hereby certify that this ~ell
abandonment record is true a.'1d exact.
Signature of Contractor or
WELL DIAGRAM: Draw a detailed sketch of the
well showing total depth, depth and diameter:
of screens remaining in the well, gravel ..
interval, intervals of casing perforations, ·.
and depths and types of fill materials used.,
Lf't)JC( .Su. r{Ac ~
Jd.',
(.,
SEP
Submit original to the Division of
and One copy to the Owner .. Env i reni'u'M')w~t~mri O ~ne
RALEIGH, NC
CD?Y to the Driller,
'WELL LOCATION: Draw a lc(!ation sket,ch s:1oh·i::c tbe d ... i.!""ecti_-'Jn aJld dista..1.ce of' the
v1ell to at least two (2) nearby refe2·ence :poir:i:ta such as roads,
intersections 2x.d strea.1119. Ide:itify roads w-.'i th 3'-t.s. te F..ighw-ay
road ident:i.fication nu.-nbers.
.. -
.. ''•
'I
,,
North Carolina
Department of Nctural Resource!_, and CcJ!:it!~.::i.ty De:velo;Jment
Di.vision cf Environmental Na11.ei21r.t~nt
WELL ABANIXlNMENI'
RECORD
P. o. Box 'Z76/!f7 -R.9.leigh, N. _c. 2'.1611
.QONTRfl.CTOR : --· .!.'~· ~'Q.'======~=
1 •
2.
3.
4.
5.
6.
7.
WELL IJXATIO.~: (Shew a sketch of the location on back of fonn.) ±M.,cl,,..,-1 # 3 ,;i_:;
Nearest Town: TroLA+ rn f'lrv County_-"::C.='-r_.::_.&.._.,_.1 ... 1 _____ _
f\J C 2-I S R I 3 I b' Quadrangle No. L lp la R lo
(Road, Comm.mity, Subdivision, Lot No.) S~""' ti J:r ½5/lc
OWNER: ?e"' I (_ lAlA')n!P/2 ER<'-eze Ex ,J LA+ '3)-41-Y> LoNq g,o-5.J-33
ADDRESS: -n:c Q~tc\ JV\ A ..J WELL DIAGRAM: Draw a detailed sketch of the
well showing total depth, depth and diameter TOPOGRAJ.'HY°:draw, slope,hilltop, valle,i:,flat of screens remaining in the well, gravel
CASING REMJVED:
feet diameter
;;i.'·
interval, intervals of casing perforations, ·
and depths and types of :fill materials used'.·
L lf,oJ_ $ U ''-..f!.»c e.
8. SEALING MATERIAL:
Neat cement
bags of cement / •->
gals. of water_L
Other
Sand cement
bags of cement
yds. of sand
gals. of water
Type material -------------·II
Amount -----------'--------11 9, EXPLIIIN ME.'I'HOD OF EMPLACEMENT OF MATERIAL
C.€ ['IPN1. rr, I xfrt (y 1➔-"-l,u $f@r A-NC~
I do hereby certify that this Kell
abandonment record is true and exact.
Submlt orlgln,,l to the Division of Environmental
and one copy to the Owner.
• _Li..1/
~l!WQ!
SEP 2 1987 ifil
GROUNDWATER SECTION Nanag=ent,RilEIG'ff:YNbo tne Driller,
WELL LOCATION: Draw a location sket.ch z!:1oi•;i::-lt tl!e di!'ect2.on a:t:d d.ista.--i.ce of the
well to at least two (2) nearby refe1·enc0 po:i.nt.tJ such as roads,
intersections and stream9. Identtfy road..s with S"ta te Fia;h-...ray
road identification rn.:..-nbers.
North Carolina
Department of Natural ReBources and C:n;;n:·i .. ::.ity Develo?m~.nt
Di.vision cf Environmental Mane.z.':!lJ!e.nt
WELL ABANOO.'IMENT
RECORD
P. O. Box ;nf:Rrl -F.s.leif.h, N. C. 2?611
CONTRAC'roR REG. NO ..
1 • WELL UX:ATION: (Show a sketch of the
I
Nearest Town: T,ou-1 :toe 01
:i:1•tt<1_e,-,t 1± 31;,$' location on -Dack of' fonn.)
County Irg df 11
_ .... rJ::-,,.(,....._[), .1..) __ .:.1.S...cR,_,..,1-"'3c..:l;;:..S'-,-----,---=---,--,,-~--Quadr~le No. L -17 (g R 1
(Road, Comm.mi ty, Subdivision, wt No.) s~~, ._, '"' :re 45~ •
I
OWNER: Pa "-\ (__ w I'~~ r 2.
3.
4.
5.
6.
ADDRESS: 'T C:Q \!, +I tn I\ ,J
TOPOGRAPHY:draw,slope,hilltop,valley~
USE OF WELL: Tg h'.l(i' o \,s DATE: g;-;;i_ h-f7
TOT.AL DEPTH: (0 0. S DIAMEl'ER: .:2.
WELL DIAGRAM: Draw a detailed sketch of the·
well showing total depth, depth and diameter
of screens remaining 'in the well, gravel , :
interval, intervals of casing peri'orationa, ''
and depths and types of fill materials uaed:
7. CASING REMNED:
feet diameter
8. SEALING MATERIAL: .
9,
Neat cement
bags of cement-1.:2
gals. of water_:1._
Other
Sand cement
bags of cement
yds. of sand
gals. of water
Type material ______________
11
Amount ·---------------11
EXl'L/llli METHOD OF EMPLACEJt£NT OF MATERIAL
(e M£ IV t m u e & l,) ,+ >--I,) A-te c a 0,1<£
, eJ we11
I do hereby certify that this ~ell
abandonment record is true and exact.
h®M~ /.,v r MU g' -3)-g' /
Signature~ Contractor or Agent Date
-------c._-;;-f\ rJO-S '-'\ 0 f,. ( ~ '
F[t'
SEP 2 1967
GROUNDWATER SECTION Submit ortglnal to the Divlslon of
and one copy to the Oi.mer.
Environmental 11an"ftAfE"ffiH,_"nlt_ co;,y to the Driller,
' i
WELL WCATION: Draw a location skgt.ch sho\•;i:;E tl>..e li°"i.!'e~t2..on ct:-:d dista..--i.ce of the
well to at least two (2) !":earl)y reference poilYt-s m;.c:l as roads,
intersections ar.d st-re-a.ms. Identify roads •••i th S'to. te I-i..i3hway
road ident.ification ni.:J1;bers.
,,, ,,..,
' .,
North Carolina
Department of Natural Resources and C...")!'",;~: .. ::.ity Developme-.nt
Di.vision cf Environmer:.tnl Ma?1c.32mcnt
WELL ABANIX1.'00!Nl'
RECORD
P. 0. Box Z,687 -Raleigh, N. _c. 2'!611
.QON'J'RACTOlL
1. WELL UX:ATION: (Show a sketch of the location on bacl, of form.)
Nearest Town:_T,._r,._o""""'..\-'-"-'""'-'A-"',.;"-------------C.cunty IR-e cl.t 11
...tlNw..c.,.&!a.!..1 --~s~· R~/L..:,=lfl'.L-_____________ Q.uadrangle No. L -(o b -p. !?
(-Road, COlllllUility, Subdivision, Lot No.) Ser,,J l'lc Ir 4582.
2.
3.
4.
5.
6.
OWNER: Pa"'' c wAo/C''"-sg n,s,
ADDRESS: :Cco,i+rnee-1
TOPOORAPHY:draw,slope,hilltop,valleyd~
USE OF WELL: 7£ °'6' o 't,s DATE: 't -,,14 -!:'?
TOTAL DEPTH: S:( ' DIAME'l'ER: 2..
7. CASING RF.MOVED:
feet diameter
8. SEALJNG MATERIAL:
Neat cement
I bags of cement I ·2-
gals. of water 9
Other
Sancl cement
bags of cement
yds. of sand
gals. of water
Type material, ______________ 11
Amount, __________ --'------11
9, EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL
c. e"" e,J-~ "'ct;!, w <&to
I do hereby certify that this ~ell
abandonment record is true and exact.
--,;,~ vv -JJ,jJ s:-51 ff?
Signature of Contractor or Agent Date
WELL DIAGRAM: Dr-aw a detailed eketch of the
well showing total depth, depth and diameter
of screens remaining 'in the well, gravel
interval, intervals of casing perforations,
and depths and types of fill materials used.-
t~,._,cf s ..... r-C.p,c..(!,
"_n • l!, .:~r,, ~
p~r
SEP 2 l867
GROUNDWATER SECTIO~
Subinit origln.sl to the Division of Envit·onmental ManageinW,,EI~ !'!o~,y to the Driller,
and Ohc copy to the 0--"'fler.
p
WELL LOCATION:
-· -.
Draw a lo.Jation sket.ch z:loh-i'::.i; the d...i..!'e:.:-ti-:in a.t:d dis½,ce of tl1e
well to at least t'\.•Io (2) r:ec.r":)y reference peint:J si;.ch as roads,
intersections a..r1d streams. IC:entify roads h~i th .S'-t.s. te 1-Iighway
road identification ni.;.."1;.bers.
Nonh Carolina
Department of Natural Re.source.s and CoPr.:~.:1.! ry Development
DJ.vision of Environmental Ma!la;,;eml!nt
WELL ABANIXlNMFNl'
REX::ORD
P. 0. Box Z7637 -F.sleigh, N. _C. 2?611
CONTRACTOR REG. NO.
·. .:t:tvc."7l f ,.J + ·31 J.. > 1. WELL LOCATION: (Show a sketch of the location on back of form.)
2.
3.
4.
5.
6.
7.
8.
Nearest Town: lrov.:-\-ro A f'l County XR-r,lt 11
....:N..;..;;c~2,'-'1'--_-"S.,;R"'--'lc...3ut.,./i' ________ ~ ___ Q:uadr~le No. L-!d, -R 9
(Road, Comnunity, Subdivision, Lot No.) sa,"' "Ir4S~4
OWNER: fq,v, I C w e~il/er
ADmESS: TY-ou+me,-J
TOPOGRAPHY:draw,slope,hilltop,valley flat
USE OF WELI,: ~ "'f O p S: DATE: \? -e: P -:f 7
TCYl'AL DEPTH: ,5t;' DIAMETER:. _ _.,.;l::..__H
CASING REMOVED:
feet diameter
:)._
SEALING MATERIAL:
Neat cement Sand cement
J.. baas of cement...12::_ bags of cement
gals. of water--9.__ yds. of sand
gals. of water
Other
'l'ype material
Amount
_WELL DIAGRAM: Draw a detailed sketch of the
well showing total depth, depth and diameter
of screens remaining in the well, gravel
interval, intervals of casing perforations,
and depths and types of fill materials uaed;
____ LSaJ:f\L!,v~l)=S ctr {:o.r €.
5'-1'
9, EXPUIN METHOD OF EMPLACEMENT OF MATERIAL •
r
1Al W-11,II
I do hereby certify that this ~ell
abandonment record is true and exact.
7--Y'r:0&tiv... \ It' , w} g'-.? 1 -,r 7
Signature of 6on'tractor or Agent Date
l~' 'f'F5'
1...d • R , C 9 ,~:ri®Jl.
SEP 2 1987
GROUNDWATER SECTION
Submit origlnRl to th~ Division of
and one copy to the Owner.
Envir~11mental Mana-liJ:GH~rffCco?y to the Driller,
,.
W"ELL LOCATION: Draw a location sketch s:1oi•;i:1;; tl:.0 di!"'ecti or:. a:t;d dista.-,.ce of the
well to at least two (2) r~€arby reference point.g such as roads,
intersections and stream~t. IC.entif'y roads i-.""i th .Sta. te I-!ighwz.y
road identification ni..:..'Tibers.
_,
North Carolina
Department of N&tural Resources and CoI;;r:!~.:'!ity Develo~ment
Di.v:i.sion of Environmer:.tal Manegc.ment
WELL ABANlXlNMENT
RECORD
P, 0. Bo::c Zl® -Raleigh, N. .c. 2?611
~~1TRAC'IUR REG. NO. . ========•=~~--===··· :t:f'l(_;-;i:. ;;+
1. WEIL U>.:ATION: (Shew a sketch of the location on oack ot· form.)
3.
4.
5.
6.
1,
Nearest Town: TV'o'-:\,4·'/Y'>f'>,J County Ir~,P,e /l
....:IV.;c..a=C...,...2:za..il __ .;;,5..:E.:....,IL,3.;w.l .,_<? ____ -,---,,--,----,---Quadrangle No. L -/,, /,;, -R / D
(Road, Con:munity, Subdivision, Lot No.) ~,,;Qc ~ :t.R. 4.;f;'-1
ADDRESS: T Roy::t:;;, fr-
TOPOGRAPRY: draw, slope, hill top, valley &
USE OF WELL:TR<:n:vf ().,\1-0 · DATE: 5?-J&-\? 1
'l'OTAL IlEPl'H: S" D , S DIAME'rER: .;:l.. ·--""'--!
CASING REMJVED:
feet diameter
.;i..
WELL DIAGRAM: Draw a detailed aketch of the
well showing total depth, depth and diameter:
of screens remaining 'in the well, gravel
interval, intervals of casing perforations,
and depths and :t;ypes of fill materiais used.·
O'Lt'le>,i<;ut+l'C'I. .
,).
8. SEALING MATERIAL:
9.
Neat cement
bags of cement 1-S-
gals. of water-3_
Sand cement
bags of cement
yds. of sand
gals. of water __
Amount __________ _;_ _____ II
EXPu:m 1-lli'I'HOD OF E1>1PLACEMENT OF MATERIAL
' JJ ' '.b'.Vj-2-w d;;A.
~ f ~
I do hereby certify that this ~ell
abandonment record is true and exact.
, ~--:ct, w, !W 'il-31-S'?
Signature of Contractor or Agent Date
Submit ,,riglnal to the Division of Envircnmental Managenent, one
and one copy to the O·..mer.
Jp)~~ITW!S!ITT .. 1 nit!l ~1~; m 2 1sa1 """
GROUNDWATER Sf~TIG:'i
co;,y t~Al.:1:i&Jli~ ¼iir'
WELL LOCATION: Draw a location sket.ch s°:JO\•;i:-i;; tb:: t:Li.!"ect.ion a..:·~d distance of the
well to at least two ( 2) ::.ear!~y reference poi::1-:.9 sJ.c!l as roads,
intersections and streams. Ic3.entify roaCs wi. th 3'ta te }li3hway
road ident_ificaticn rn;,nk)ers.
-...
.,.e.c..·
l.ZJ:"IDJ .:::;-9CfV'
I
J <,.., .,
NORTH pAROLINA DEPARTMENT OF NATURAL RESOURCES ANO COMMUNITY DEVELOPMENT
DIVISION OF ENVIRONMENTAL MANAGEMENT -GROUNDWATER SECTION
FOR OFFICE USE ONLY
P.O. BOX 27887 -RALEIGH,N.C. 27611, PHONE [phone]
WELL CONSTRUCTION RECORD
DRILLING CONTRACTOR _,_,lll'-'R.'-'-"c_Q..,__ __ -_,_C"-'-"@-"o-""'-',.,-'J"--"'l,-)-'A.,_-1-_,,>'-'r
DRILLER REGISTRATION NUMBER __ l~O=()~O~-----
1. WELL LOCATION: (Show sketch of the location below)
Nearest Town: ·TR ou:\-t:n AN
Su;moNS s.e,r1,·, TA,-1)< SR /3~3
(Road, Community, or Subdivision and Lot No.)
2. OWNER >iA±f Q~ ;Jc_ g 19£~00§" S trl:c Ti9,J}:-
ADDRESS (l /1.c) wl\l ,P .JA-/-f 'l. Q · (Street or Route No.)
0_1+lf ,91..
City or Town State Zip Code
3. DATE DRILLED f(-)-f-J'7 USE OF WELL re me Q b c:. • 4. TOTAL DEPTH -~3~4 __ CUTTINGS COLLECTED □ Yes □ No
5. DOES WELL REPLACE EXISTING WELL? 0 Yes ~ No
6. STATIC WATER LEVEL: 34,I{° FT. 0 above TOP OF CASING, 18" below
TOP OF CASING IS / · '-/ 7 FT. ABOVE LAND SURF ACE.
7. YIELD (gpm): NII METHOD OF TEST 8.q I l
8. WATER ZONES (depth):--~~~~-----------
9. CHLORINATION: Type -~,V~fl~_ Amount NII
10. CASING:
Depth Oiamet~r
Wall Thickness or Weight/Ft.
From ~Q'""-__ To ,2</ Ft. __ ;). __
From ----TO ___ Ft. ___ _
From To ---Fl.----
11. ·GROO I.:
Material
g,,.,i,,-,;e Depth Material Method
From -~C)~-To .,}J.,i.,, Ft. ¾f"'/1,/~
From ____ To ___ Ft. _____ _
12. SCREEN:
Depth Diameter Slot Size Material
From ;)_ 'I To S if Ft. ,2. in .. o,;,o in. Pt!C..
From ____ To. ___ Ft. ____ in. ___ in.
From ____ To ___ Ft. ____ in. ___ in.
13. ,QRA>et 'PACK: 5,1),vcl ·
;2), ft,
From ::£:-
Depth :J'{
To pt. Ft.
Size
rneJ
Material
From ____ To ___ Ft. _____ _
Quad. No. L ~? fj /fl, Serial No . .II:. 41, 7~
Lot 35 43 oil, Long. So $S 08 Pc __
Minor Basin _____________ _
Basin Code _____________ _
Header Ent. _______ GW-1 Ent. __ _
mw tr 3
STATE WELL CONSTRUCTION
PERMIT NUMBER:
County:
Depth
From To
DRILLING LOG
Formation Description
If additional space is needed use back of form.
LOCATION SKETCH
(Show direction and distance from at least two State Roads,
or other map reference points) 9 • #
3 3
Jg
~'-SlP~:c
?,-1">
"' .,_
D ,,it
woob
·,
.j. ,h,& ~ ! TR.A:,,,._ ~
D
SR I 333
14. REMARKS:----------------------------------------------
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15 NCAC 2C, WELL CONSTRUCTION
STANDARDS. AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDoD TO THE WELL OWNER.
~~wt NAHJREOF ONTRACTOR OR AGENT DATE
GW-1 Revised 11 /84 Submit original to Division of Environmental Management and copy to well owner.
•
NORTH CAROLINA DEPARTMENT OF NATURAL RESOURCES AND COMMUNITY DEVELOPMENT
DIVISION OF ENVIRONMENTAL MANAGEMENT
Lithologic Log Quad No • L (p 7 Ci / ~ 0
Log by: :(1 )'.'<) "''1 H ,LL Date S'-;q; -Y°' County Ir-e Jell
Serial No •. :X::R 46 7<;
Location, Town ~o~-1-r>-A rJ Lat. 3S43o;t Long. 'i;O S!i OS
Owner >.i9r•,p"' Sfp+:c. :ffrr>K Driller T, l--l I L-L Date Drilled i -,)<J-f;?
Depth '-'-I ft.: Diam. Ct,-"!t in.: Cased to 3 V ft.: Elev. ___ ft. above MSL
Cuttings ________ ...cElec. Log, __________ Garnma Log, _________ _
Type Log: Drillers, M.icroscopic, Macroscopic ( circle one)
Description
El. 0
l'\,., ,
' r O, . ·
V
fl,,_ 4. Ill If D11., • (I ( 0 · "
5C1<-e_e,f\} ;;i, L/ -3. 'f
r u;. O-.:Jl/
~Prr' cP ")?,IA -39
fh,....__J) !' -0 ~ ;:;, ::i, fo
-
Depth (feet
from to
r) L/
t./ q
'f' I Lj
/'-( JC,
,:;4 J. 9
}-2),..,
~ hA9'
Thickness Drg. Tim,
(feet) (min.)
/,<-+-<:a I +-<:. oo"' Ci , ':/ I'
'
I JO, • (_ d .,,__..,__,-,
' ,;2. ) " ' ~,
I .5
f----------------------1----1----1---------1------1·'
'--------------''---.....L----l.------L-----'
GW-2 Revised 10/1/80
\ I
( .. ¥! ' \ .. f .. ;
,;.
Lithologic Log (con't) Quad No. ______ _
Serial No. -------
Description Depth (feet) Thickness Drg. Time
from to (feet) (min.)
.
l
'
•
NORTH CAROLINA DEPARTMENT OF NATURAL RESOURCES AND COMMUNITY DEVELOPMENT FOR OFFICE USE ONLY -. DIVISION OF ENVIRONMENTAL MANAGEMENT -GROUNDWATER SECTION . ..
-P.O. BOX 27687 -RALEIGH,N.C. 27611, PHONE [phone]
WELL CONSTRUCTION RECORD
DRILLING CONTRACTOR _ _,{IJ,,_1_,_,R...,<'..,_/),_ _ _,_G,._.,-R"-o"-'u,,_,.,J=_,,w""· A-=.,_-N'-"r'-----
DRI LLER REGISTRATION NUMBER --~/O=Q'-'-"0 _____ _
1. WELL LOCATION: (Show sketch of the loca1ion below)
Near~st Town: ]·Ro,.clv:n er aJ
Si'/"10ell S•fd;, Tuollc ~R 13'3 '?
(Road, Community, or Subdivision and Lot No.)
2. OWNER s te tee of II/ c .$ 19 mcN.!.· Sf'f~ • < TA,"/;,
ADDRESS Cdcoy 111c9wA-\.!'~ • (Street or Route NoJ
City or Town
3. DATE DRILLED fs-r).,·87
Zip Code
USE OF WELL 1R mo ObS ,
State
4. TOTAL DEPTH 3'/ CUTTINGS COLLECTED □ Yes □ No
5. DOES WELL REPLACE EXISTING WELL? 0 Yes ~ No
6. STATIC WATER LEVEL: 3/ • / 9 FT. 0 above TOP OF CASING,
~ below TOP OF CASING IS /, '17 FT. ABOVE LAND SURFACE.
7. YIELD (gpm): -~rJ~/t~--METHOD OF TEST __ 8~11~1_l ___ _
3. WATER ZONES (dep1h): --""--'L---"3'-''-/'-----------
!l. CHLORINATION: Type -~N~fl~-Amount NII
10. CASING:
Wall Thickness
Depth Diamet~r or Weight/Ft. Material
0 From-=--To ,.)'I Ft. .,?. /?.ti(
From ___ _ To Ft.
From ___ _ To Ft.
t t. -etl(')t1.T':
8-P,v-l-o,.,,h Depth Material Method
Quad. No. L b?5 17 Serial No . .Ig '/67'1
Lat 35' 43 o;>. Long. 8 b SR ~Ii' Pc __
Minor Basin _____________ _
Basin Code _____________ _
Header Ent. _______ GW-1 Ent. __ _
34)2
STATE WELL CONSTRUCTION
PERMIT NUMBER:
County:
Depth
From To
DRILLING LOG
Formation Description
GROUNDWATER SEcr · ION RAI EIGH 'IC • j
If additional space is needed use back of form.
LOCATION SKETCH
(Show direction and distance from at least two State Roads,
or ·other map reference points) p ~; ~ 1'1
/2\,rf :, V ! -(!>~b
From ~0~-To :2 I Ft. Af P<lleh po.n,J! ,.,.,; w11-1-,a
addeJ From ____ To ___ Ft. _____ _
12. SCREEN:
Depth Diameter Slot Size Material
From JI./ To 31./ Ft. .l in. ,O:Zt! in. E_vC
Fr;)m To Ft. in. in.
From To Ft. in. in.
1l ~~~JL PACK
Depth Size Material
D
From ::;. L To 31./ Fl. M..(J S R 1.333
From To Ft.
1,i. REMARKS:
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15 NCAC 2C, WELL CONSTRUCTION
STANDARDS, AND THAT A COPY OF THIS RECORD H~~IDED
1
T,q JljE WELL OWNER.
-; _,. ~ !.iM:e._ g ~ 31 ~ J-'?
SIGNATURE OF CONTRACTOR OR AGENT DATE
GW-1 Revised 11 /84 Submit original to Division of Environmental Management and copy to well owner.
..
NORTH CAROLINA DEPARTMENT OF NATURAL RESOURCES AND COMMUNITY DEVELOPMENT
DIVISION OF ENVIRONMENTAL MANAGEMENT
Lithologic Log
Log by: T1 '('(' C!'"-' \.4-1 LL ( Date County ;:fre cQ~ ( I
Quad No. L {,7 f) /'?
Serial No.fl '16 7£
Lo cat ion, Town I !Ro IA.ti::') A r-l
Owner $ '? "'o"' sf /f:f; c :re-,-, )c
Lat. J.5" 'I 3 o,;2. Long. j<'O {R o Ii'
Dr i 11 er __ ~-J'--_b),=.,,'-"'L....:l:;._ _ __;Dat e Dri 11 ed _ __.x'.,__-"';)-")----"· ~'--7----'
Depth._..::;3c..Y:.___ft.: in.: Cased to 3 '/ ft.: Elev • ___ .ft. above MSL
Cuttings ________ Elec. Log, _________ Gamma Log, ________ _
Type Log: Drillers, Microscopic, Macroscopic (circle one)
Description Depth (feet Thickness Drg. Tim,
from to (feet) (min.)
1)1? I/ .n,,., u r : I 1:1 . .., /'J u •10,, J,-f cooo,,J
L, ,.,1,_'+ D, .o +o f, rv 1c I'\ r., L, r I .._ lf 9 r::.~5'-j-c-~}, f ' !Ooo,. r.:,, l
, 1/, I , Ci I 1./ L, a.J,.J-. l?n fl T11..1 ,J_ 1 ,,, / Ow f'\D 1., ( j A-,
--f) ,,,J.,_ ,. -s, n/ r a_.
,
)'--; 19'
Tl,., i Ta-.C ·n u-Jq ,:iy
l)An_.r l"'-,J • ( 9 . { JA-.,, ...,,.,, _,. -\ ~ L/ .;t q
f),, A 1 r /). ·-,;).. q Mo,..s+ Tr, .3</ /...fH-1-$ Pl I+ i.l?oo,v u --,;-;;i,17,>0~1f'':"l''lll
ill ~\ t;,./113.!.,\ ~ It' : l ,, ,, I,
IU\ll"' •·'! \~ ..
I,.,~
e!!I ~ SEP 2 J):lO I
. I_,,'""'' H,R S£.CilO ' , \l ivc1•~vn•i" i:!GH, NC
$ c.12. _., e ,., ;;) '-I -s 'i I 10/ ~c ~~e,.J
(' .5, 9 o-,;:,'-( ;;i_ I o ,.
I s'
S, /}-rJ tP 'l/-3'-1 1-~ -( ,,,.,J
r,,, 1) f) -2 I -,.J_ ....
.
GW-2 Revised 10/1/80
Lithologic Log (con•t) Quad No. -------
Serial No. ______ _
Description Deoth (feet) Thickness Drg. Time
'\ from to (feet) (min.)
. . .
.
,
.
..
NORTH.-CAROLINA DEPARTMENT OF NATURAL RESOURCES AND COMMUNITY DEVELOPMENT FOR OFFICE USE ONLY '\; , ..
DIVISION OF ENVIRONMENTAL MANAGEMENT -GROUNDWATER SECTION
P.O. BOX 27887 '... RALEIGH,N.C. 27811, PHONE [phone]
WELL CONSTRUCTION RECORD
DRILLING CONTRACTOR __,_l))-"--"'l!."'C'-'1)"-----"G--"!2"--'D'--'u'--""''-''L~ "'w'-'-"'----.\-'----~'-'fL.c.__
DRILLER REGISTRATION NUMBER --~'o~o=o _____ _
1. WELL LOCATION: [Show ske1ch of the location below)
Nearest Town: Tg,o 11 + a, A tJ
s,1e1e,.,s S''f6·c IA"1k SR 1,,:s3
(Road, Community, or Subdivision and Lot No.)
2. OWNER $fat,, Dr NC.. S •'j'mo;J5 Ser/ :c 1/JrJJc
ADDRESS lrCDµND wA+-e,-
. (Street or Route No.)
D -}-e h_
City or Town State Zip Code
3. DATE DRILLED I?-,l-'1-?7 usE OF WELL :feme ob$ ,
4. TOTAL DEPTH 3 'I CUTTINGS COLLECTED □ Yes □ No
5. DOES WELL REPLACE EXISTING WELL? 0 Yes ill No
6. STATIC WATER LEVEL: .)7 ,5;2. FT. □ above TOP OF CASING,
,,,, t;sJ below
TOP OF CASING IS / , 9 > FT. ABOVE LAND SURF ACE.
7. YIELD [gpm): --~N~II ___ METHOD OF TEST __ 13_,,_:_1 ___ _
8. WATER ZONES [depth): --~:J~'-/~--•~s_y~•---------
9. CHLORINATION: Type -~lll~fl~-Amount /I) I/
10. CASING:
Wall Thickness Depth Djamet~r or Weight/Ft. Material
From ~Q~ __ To .21/ Ft. ;2. ___ f,/c
From ----TO ___ Ft, ___ _
From To FL----
11.GREltir.
/S,11,J/~.,,;11..f. Depth Material Method
Quad. No. L G 7 'J l l, Serial No . .,JR '-I I, 73
Lat. 35 'i 3 OY Long. S,O 58 O/i' Pc __
Minor Basin _____________ _
Basin Code _____________ _
Header Ent. _______ GW-1 Ent. __ _
M vJ Fl I
STATE WELL CONSTRUCTION
PERMIT NUMBER:
County: .IR1ecle I'
Depth DRILLING LOG
From To Formation Description
-~\l!F!lf?!l,~c\1-'1 ,~\~~,H~lFl~-~I ii'~],------
:;;1t'-.1il 'U r;,,,, , il
------'S.J:EP 2 198,
GROii NDWAiffl SECTION
---4R~ALEIGH, NC
If additional space is needed use back of form.
LOCATION SKETCH
(Show direction and distance fro at least two Sta1e Roads,
or ·oth6r map reference points)
From -~O~-To ,;) 1,:,' Ft. ¾,p,;/d,.; Pou ,,.,,0i,.,,,.1,_ wA-1,,,-,_
;;ddM 0 From ____ To ___ Ft. _____ _
12. SCREEN:
Depth Diameter Slot Size Material
From ,) Lf To 3 Y Ft. ,,2 in. -Old in. ?t!L
From ____ To ___ Ft. ____ in. ___ in. __ _
From ____ To ___ Ft. ____ in. ___ in. __ _
13. ~RAVEJ-PACK: s,1-,.,-& Depth Size
From .}!,{ To 3'/ Ft._~/1/~~~j} __ _
From ____ To ___ Ft.~-----
Material
IA:,oo & ....
S h-t& l t,~l'ltller
~ '
o._s.:,f,1t0<"1J
Si'f>-i, c.
SR l 333
14. REMARKS:----------------------------------------------
1 DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTE.D IN ACCORDANCE WITH 15 NCAC 2C, WELL CONSTRUCTION
STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED T THE WELL OWNER .
..-.---Mn$ ' 8-3J-f7
SIGNATURE OF CONTRACTOR OR AGENT DATE
GW-1 Revised 11184 Submit original to Division of Environmental Management and copy to well owner.
NORTH CAROLINA DEPARTMENT OF NATURAL RESOURCES AND COMMUNITY DEVELOPMENT
DIVISION OF ENVIRONMENTAL MANAGEMENT
Lithologic Log
Date 'i(-"--'-f_ &-7 County :Jl?ede_}J
Quad No • L -~ 7 ~ / G
Serial No.IR '-11,,73
Location, Town :IRo,,,f('l.fr,J
OwnerS1ym•N ~j.; c :tao1k Driller T-/-l-1LL Date Drilled B-J Y-t?
3 1.J . 1..f, Depth I ft.: Diam. u, -, in.: Cased to _..._.,___. 5</ ft.: Elev. ___ ft. above M,SL
Cuttings ________ Elec. Logc__ ________ Gamma Log, ________ _
Type Log: Drillers, M.icroscopic, Macroscopic ( circle one) J) -I
Description Depth (feet Thickness Drg. Tim•
from to (feet) (min.)
ir.-. . -. +:,. \'\ nn Ir Po O r O. 0 u ...,_..., cd~+ c,,... n-1
f'lnnv f?p,fl f)o' f In.-, , ,J_o --V. ,J r /,,. I ()p,1 L q I,.,_._ SIP. I J. ~ oo,.; r;,, I.J_ --r 1-\-,J l)(l.L; ' (_/ LL,~ ' -0, /'f
' (__I ,L 1 Arl T\Rv IL/ 19'
fl> I
/ I q '.">.'-( nR.u r I r.
MO I,-/-IP ,J cl~ .;) l/ ~ ';
t,,.>¾ T~ rOL_ ;)_ 9 3'-f rt"{) ,=l,-1-<: ~ '~ 0 \) 7j) .
~ -;;::;.0.l'i~Yf,\i]ft;, ~
/-10 I i}/ W&11~~"'· '1) ~l ill\ -5, ".f!P.N ~? -~-~, '._,.t
.:J-10' ~\' ""' ~!I. .. ···-.--,
I -S' -Sffl' ;.~: ....
.
~C,R,€,etJ _,IJ-3. 4 ,. "II N,DWJJ Ht $W \\ \l~ 'f
' C~7 .) '-I -0 IR'MLJE)\~trt\,, I~~
,,'
S <l.tvcf :21-s ?LI -,.]_ ~ .or.
"'I.\.Al ,.,,_c-o ' b "'-D ,
GW-2 Revised 10/1/80
•
Lithologic Log (con't) Quad No. -------
Serial No. -------
Description Depth (feet) Thickness Drg. Time
from to (feet) (min.)
.
'•
,
..
·-
~~/ ,.
NORTH CAROLINA DEPARTMENT OF NATURAL RESOURCES ANO COMMUNITY DEVELOPMENT
DIVISION OF ENVIRONMENTAL MANAGEMENT -GROUNDWATER SECTION
FOR OFFICE USE ONLY
P.O. BOX 27887 -RALEIGH,N.C. 27811, PHONE [phone]
WELL CONSTRUCTION RECORD
DRILLER REGISTRATION NUMBER --~~•=o~-----
~ 1. WELL LOCATION: (Show sketch of the location below)
Nearest Town: I R.0-.).-~ f\N
S,c,1M.Ql-.)S s~jlr\ c.. Tu~ Ti:-,::,p~ ·.\:( 3"12'2.
(Road, Community, or Subdivision and Lot No.)
2. OWNER l\l i<. C..I) ,-C--r'R.pu'-ltl •••"•1Q
ADDRESS i) 0 · eox '2 ... ."[{c, 67 \J (Street or Route No.)
JS, l'\U:7_ E..-tt-t--l -C... 2. 76((
City or Town State Zip Code
3. DATE DRILLED fi -25-87 USE OF WELL Te,"\> Db S
4. TOTAL DEPTH 39.~ CUTTINGS COLLECTED □ Yes ~-No
5. DOES WELL REPLACE EX~[,s;<¾-ELL? 0 Yes !B-No
6. STATIC WATER LEVEL: .....,._,.... -,-FT. 0 above TOP OF CASING,
,, ©'below
TOP OF CASING IS {'J./7 FT. ABOVE LAND SURFACE.
7, YIELD (gpm): t-.J/A METHOD OF TEST __ N~/~fl..~---
' 8. WATER ZONES (depth): --S~A~i-~u~(l.="-~'-ct_@=-~3~2-_____ _
w& <2 ~7 1
9. CHLORINATION: Type IJ/A--Amount --"'~/.~14~---
10. CASING:
Depth
From __ 0=--_To ?-'7 Ft.
Wall Thickness D,iamet~r or Weight/Ft.
403<'."
From ____ To ___ Ft. ___ _
From To Ft----
11..,GROOT:·,\_
Material
1),1),(,
Quad. No. I,. ~ 7 'j
Lat.35 '--13 oG
I 5 Serial No. r;e '//. ]l,
Long. Ro -5, C~ Pc __
Minor Basin _____________ _
Basin Code-------------~
Header Ent. _______ GW-1 Ent. __ ._
~,vc,
STATE WELL CONSTRUCTION
PERMIT NUMBER:
Depth DRILLING LOG
From To Formation Description
-·. . ,.
P.,t.,v.Jo,-, /'J .t , -, . -',I;, , .
,O I
:31-5 A,.JJ'
' -,.n,• -i -? liTh"\ ~-
!\ '{U I "':!• )f' i• I I,\ .
'Q;·
-@ti~"S;=;EP 2 198-1
-~0~1:J-N""DW /1. 1 £.B S£,C1 IO M
GR "ltti-1 E\-G\4-, ....,tilC~------
11 addiAfhlal space-is needed use back of form.
LOCATION SKETCH
Sef'.,,., C..
!)e~'-" Depth Material
From __ O __ To ')_b,t,, Ft. -fg '"',!ZS Pe\\e,½
From ____ To ___ Ft. _____ _
12. SCREEN:
(Show direction and distance from at least two State Roads,
or ·other map r~erence points~
.,._1\. ,,.,--?•, s
Method ~
~ouR.. 1,>/ W4/.tll-' rc,tJ&,l) -. 50 I
--wo0J) \l
' Depth /
·From J...1 To 'j,<f Ft.
Fr8m To Ft.
From To Ft
13. GRAVEL PACK:
Depth
From J-Je .I,, To S1,V FI.
From To Ft.
14. REMARKS:
Diameter
?.t"-' in.
in.
in.
Size
[,'f,_{.,,
Slot Size Material
,0'2--in. f>.V.C
in.
in,
Material
,,., 1\5 l:l -'fi\.ll'J
5,;E:!) )._
~ "I
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTE.D IN ACCORDANCE WITH 15 NCAC 2C, WELL CONSTRUCTION
STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER. r~ 1;,w
SIGNATU~TRACTOR OR AGENT DATE
GW-1 Revised 11/84 Submit original to Division of Environmental Management and copy to_ well owner.
., •
NORTH CAROLINA DEPARTMENT OF NATURAL RESOURCES AND COMMUNITY DEVELOPMENT
DIVISION OF ENVIRONMENTAL MANAGEMENT
Lithologic Log wd / # L/ Quad No • L b ~I !] I 9
Log by: T, m my )J, l l Serial No.~ '/r 7/,,
Date S(-.;2..)r &"?county file de//
Location, Town Jt2t!J vff m A ,y
i ...::, lDIN 1 2,4 2. Z.... -Lat.3SY3o(,Long. 8051: o(
Owner s,7010,J se.p:h (, TAc! /c Driller __ y;./...-'-,~Mw..:.1...:l.c....=cc.._ __ _;Date Drilled @-2. ~-8 7
3a ' / .Ly Depth ,.O ft.: Diam. _ __,.!_!2"'-,._ ___ in.: Casedto 39 ft.: Elev. ft. abo·veMSL -----'
Cuttings Yes "'-l'loos,e, Elec. Log, __________ Gannna Log, _________ _
C (,.owc.15T)l3<Md/-
Type Log· Offii~s7Microscopic Macroscopic (circle one) p I/ ' ' -U/' q ~
Description Depth (feet Thickness Drg. Tim,
from to (feet) (min.)
CJf:.LlMr,. IT. I>/VI 7-"1<1/ ,,-,,,,-.~•,-"'/ Mir Sll.lY Ct..f.1-V D .f d
r
(
,: f. 6,r~r,d '7-j)R.. Y ,(,SIJ/Jteo,,, u;) : :.~ iV//, ,', ,,. ··;: T -
J T 8,,.a,,,,; ~ /~.) -7/J/V :SLJ, C.J..l4YFY ,-.,,tJ -c,sc. :w6Y l1tt'-::.tiJ 10
l <"ii' /,o,,.y. ,-;.">J,US -(,i)ey .:::S11iJl.bi.,vr
s llr>t E ""' IJ/',(>t,Xl_ -l)_(y -/1• I 4---
LT /?~ .. .Ill N/(., 5lLT'Y F/ -ptt-"Z) :YJN/) -1)12'/ -/4-17
511111 € (Mo,, rl 17 2.L1
)4t,/. ,., JfJr,{ d fY(.. 8RN M(C., · 0tL7Y /0/ -M Cl) SA,-,0 :z.a.. ,_r
-,/ REJ./C.. S7,zr.,e.,1;/2.1o-( />10/S TI ,11 ,-fi'l ~'if"', !i\
~•Mt: (£_ 3:2. ) ( Y'rT,) A-'f .?,LL • "'~ rll{ /111'&\\ '· JI \\( \t "'· .,1 \ ;r-,,\.;JI-. ' . 5rJ(IVJ€ -(,;l'l T) 34 37 v.11 i,,';, ,
J Af11F 5LIMj);c(} A< Pw, R ~li'NS1<.r-,AJtS. OF 3 7 37 l\1 .. ---., )1181 ... -<:.fC,1\()~ 7,4N, ·,, •L.1171· &..K R/,-, , 07,.., <".N£/SS -,
1o, ,-,... r., ' ~o, .o "of\\)¾\)~~".'' 1 \'\G -\{1\\..1-'
3 )'. ) 0
,,
CA511J,E.. r'J 2'7 _.__., l' ' '
1 , B~,u,,,~ 0 Z<o <o
' Sc.11..t-r--'
,--39 ..... I> !<.to 2...9
' -A. l::,n.a 5 :s.f><"-lll 21!,.(, J'!
"
....
. .
GW-2 Revised 10/1/80
'•'I
Lithologic Log (can't) Quad No. -------
Serial No. ______ _
Description Deoth (feet) Thickness Drg. Time
from to (feet) (min.)
'
I
.
'
.
.
'
.
• I
' . • I . ~
I ·.,
. ,.
. '
GEOPHYSICAL LOG
NORTH CAROLINA
DEPARTMENT OF NA TUR AL RESOURCES
AND COMMUNITY,: DEVELOPMENT
DIVISION OF ENVIRONMENT AL MANAGEMENT
GROUNDWATER SECTION
Log by DSC.A.I<.
StG,Mfl.N Location
TRl'.ult-,\~, N.l.
Date
¼ ~.R. 1333, 4M\LE
Owner __ G_w...c...;.cS _______ _ Driller \,\\LL
Depth ~9 ft. Dia. 2 in. Casing _3=-°t_,___
LOGMASTER
f I.
Potential __________ _ mV/in. Potential
&, 7
L
Log No.
Vicinity Map
1720
Well Serial No. U 'd2tf
Well Quad 'No. L-<,,,j/j
IN<'...-¾f ~'t22 WELL 4 3S t3
County :tREt:>£LL 'I~' s~
Date Drilled 3-7.S-81
Elevation ____ _ ref. MSL
WIDCO
mV/10 div.
Resistivity ohm-m/in. Resistance ________ _ ohm/10 div.
PR Logging Rate ______ _ ft./min.
Gamma ___ I D..;:__-2~5 ____ _ Counts/sec.
T.C.
Gamma Logging Rate __ \:..:lo=--__ ft./min.
Remarks
. _j_ ..!..' l ·"
PR Logging Rate _______ _ ft.Im in.
Gamma ____________ _ mR/hr.
T.C.
Gamma Logging Rate ft./min.
Remarks
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GEOPHYSICAL LOG
NORTH CAROLINA
DEPARTMENT OF NATURAL RESOURC!:S L
AND COMMUNITY DEVELOPMENT
DIVISION OF ENVIRONMENTAL MANAGEMENT
GROUNDWATER SECTION
Log by DSC.A.R \-\c:.wA.R:D Date
Log_ No.
Vicinity
',720
Map:
1123
Well Serial No. :r,e lfl'lS
Well Quad No. l-l.. 7; /g"
Location INl.::\f ~'IZ.2 ww.i3 3S f3 'SEPTll. Tf\1\lK. SE"R. County __,:I::=="12£==b=E""' =------~r;, s-r Som\\ S\Dt. DV S.R. \3ss. 1/'1M\Lt I~~ r\E \ D TRl),\fTMAl\l i l'l.C..-DN. ' , l\)Qo wcs1
Owner ulC.. Driller Date Drilled 2,-2S-S1
Depth °?>'-\ ft. Dia. '2 in. Casing fl. Elevation ____ _ ref. MSL LOGMASTER WIDCO
Potential mV/in. Potential mV/10 div.
Resistivity ohm-m/in. Resistance ohm/10 div.
PR logging Rate _______ ft.Im in. PR Logging Rate.--------ft.Im in.
Gamma 2'S-'SD-IDD Counts/sec, Gamma mR/hr.
T.C. T.C. -~
Gamma Logging Rate __ l~lo~ __ f I.Im in. Gamma Logging Rate
Remarks Remarks
GEOPHYSICAL LOG
NORTH CAROLINA
DEPARTMENT OF NATURAL RESOURCES L
AND COMMUNITY DEVELOPMENT
DIVISION OF ENVIRONMENT AL MANAGEMENT
GROUNDWATER SECTION
Log by _D==~=A--'-'l<-'----=-t-\=D.N~A.:..:..Rb=--
Location
1R~\HMfl.l\1
Owner G-ws
Date
Driller
8-25-Bl
Log No.
Vicinity
1720
Map
172"2.
Well Serial No.
Well Quad No. L-fo1l'J/(;
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-, IM. \:\\LL Date Drilled
Depth ::>4 ft. Dia. 2 in. Casing _3=-lt...,___ t t. Elevation ____ _ ref. MSL LOGMASTER
Potential·-------~---'--"-mV/in.
Resistivity ohm-m/in.
PR Logging Rate ft.Im in.
Gamma Counts/sec.
T.C.
Gamma Logging Rate ---'-\-"b ___ f t.l min.
Remarks
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Remarks
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GEOPHYSICAL LOG
NORTH CAROLINA
DEPARTMENT OF NATURAL RESOURCES
AND COMMUNITY _DEVELOPMENT
DIVISION OF ENVIRONMENTAL MANAGEMENT
GROUNDWATER SECTION
Log by bSCAR l-lDw.l\RD Date
E.UFOLI\
l
Log No.
Vicinity .Map
172.\
Well Serial No.
Well Quad No.
C. i<c-,SS-K.Dllu::,5
I
L-t,,l g/7
INC..~~422 WE.LL ,W2. 35 43 C'Z..
Location ~\CsN\ON SE'!"TlL 11>..N.°K. 'SE?-. County --'I='-'R,,,E,:,D<-::E:::L=a\_=.. ____ _c.,.;.::••W' s-r C' Fr
~ :rF,r,.uJMPlN. 1 t,\.L .-[),.I $11\ffil. 51Df. t.r SR. L"333 , Yl.f ""'Lt: 1N '81\tK FlELD , 1000' W£~T of" S.R. \Dc.4 Owner bw 5. Driller Date Drilled 'D-""2.S-81 Depth ft. · Dia. 2 in. Casing ~J~4.___ fl. Elevation"'-------,.
ref. MSL LOGMASTER WIDCO Potential __________ _ mVlin. Potential mV/10 div. Resistivity ohm-m/in. Resistance ohm/10 div. PR Logging Rate ________ ft./min. PR Logging Rate
Gamma Counts/sec. Gamma mR/hr. T.C.
T.C.
Gamma Logging Rate _ __,_I k.=-__ f t./m in. Gamma Logging Rate ft./min.
DIVISION OF ENVIRONMENTAL MANAGEMENT
GROUNDWATER SECTION
May 27, 1987
MEMORANDUM
To:
From:
Rick Klingel, Mooresville Regional Office
Tony Parker
Subject:
Jay Bennett, Technical Services Grou
Proposal For Drilling Assistance
Sigmon Septic Tank Service Subsurfa e
Investigation
Incident #3422
Iredell County
This memo is in reference to the proposal for Drilling
Assistance received from your office on May, 1987.
In order to expedite your request please resupply the
following information.
1) Type of contamination expected -A more specific
identifier of the chemical constituents to be
expected. This will allow the drilling crew to
plan for safety precautions at the site and to
bring the correct material for the well
instruction.
2) A Base Map of the site-Showing the locations of
the proposed monitor well locations, any overhead
or underground utilities near the monitor well
locations as verified by U.L.o.c.o., the potential
source(s) and the impacted wells, if any. Please
insure that the map has a scale of at least 1" = 100'
or less.
Note: The drafting dept. (Larry Goodwin) can
assist in preparing a base map.
3) Utilities on site (item #9 on the Drill Plan)
verification that all utilities have been cleared
(overhead and underground) by U.L.O.C.O., etc.
Note: The magnetic & cable locator is available
to you upon verbal request to Keith
Edwards.
If you have any questions or need assistance please do
not hesitate to call me.
JB/bb
cc: Jncident Files
.. ...,., ..
POLLUTION !~PORTING FORM
1. Incident +3,./.(d:J, MAY 1 3 ffiB?:: Division of Env1ronmental Management
2. Tabulate only ___ _ GROUND WATER SECnnN
IWF!f8HP~. t C TIO N
GROUNDWATER SECTION
A
B
1. Emergency response @ Complaint inv~stigation 5. Re-evaluation : #
2. Compliance investigation 4. Routine inventory 6. Other :
POTENTIAL HAZARDS (i)Toxic chemicals 2. Radioactivity 3. Air emissons 4. Explosives 5. Fire
Incident Name
Address
County
-:t::'t-
·Name
k e.
~pany Agency
..L->.-.. d~tl C ....
Briefly Describe Incident
~ l I S -1-<
,<..<,,<..,r
INCIDENT
City/Town
.s -1 ... -1., .... ;
Region DEM Regional Contact
J;.,
PERSON REPORTING INCIDENT
Date Time
8'7 f
Telephone
REPORTED BY: 1. Responsible party overnment agency 3. Private party
RECOMMENDED ACTION
1. Investigation complete 3. Initiate/complete cleanup 5. Technical support 7. Enforcement action
2. Continue investigation 4. long-term remedial action @Drill crew 8. Monitoring plan
Comments
4 h. G-w· "
.,.,, L.c..sou"'I
LAB SAMPLES: 0 Yes 2. No
Signature Date
GW-61 Revised 11/85 North Carolina Department of Natural Resources and Community· D
POLLUTION INCIDENT REPORTING FORM Incident # __ _
County: J:",J._q
POLLUTANTS INVOLVED
MATERIALS INVOLVED AMOUNT STORED AMOUNT LOST AMOUNT RECOVERED
E
IMPACT ON SURFACE WATERS
&No
lDistance to Stream (ft)I Amount in Water (gal)
WATERS EFFECTE.D 1. Yes No([)Potentially ~l)d,
F I Name of Stream I st7eam Class FISH KILL: 1. Yes {} No tll'I 1'14,-. ./
RISK ASSESSMENT
Use these Codes: High= 3 Moderate =2 Low =·1 None =O
Resource Threat GROUNDWA TEA Amount lnfiltratin·g Land
Vertical Migration of Contaminant ~ Horizontal Migration of Contaminant
Areal Extent of Contamination SURFACE WATER AIR
Probability ol Violations -3 l) D
Remedial Action Priority I ,~ CJ
G Potential Hazard of Substance l. " I,
Threat to Drinking Water j (> 11
Seriousness of Threat .:l.. " ()
Overall Regional Concern j__ ;J 0
Please Circle the ApproprJate Response(s):
1. This ·Incident poses additional threat to human health by: (1) inhalation (2) absorption (3) ingestion
2. This incident poses additional threat to the envlron.ment by potential adverse effects on :
(1) sensitive areas (2) wildlife (3) fish
POTENTIAL SOURCE OF POLLUTION
SOURCE OF POTENTIAL POLLUTION TYPE OF POLLUTANT LOCATION SETTING
1. Intentional dump 9. Sewer line 1. Pesticide/herbicide 1. Facility c:/> Residential
\g) Pit, pond, la,,2,.00~ 10. Stockpile 2. Radioactive waste 2. Railroad 2. Industrial
3. Lea k--unde rground 11. Landfi II 3. Gasoline/diesel 3. Waterway 3. Urban
4, Spray irrigation 12. Spill --surface 4. Other petroleum pi-od. 4, Pipeline @Rural
H $ Land application 13, Well 4flx,e wage/septage (;)Dumpslte
• 6. Animal feedlot 14. Dredge Spoll 6. Fertilizers 6. Highway
7. Source unknown. 15. Nonpoint source 7. Sludge 7, Residence
8. Septic tank i Solid waste leachate 8. Other
Metals MULTIPLE SOURCES AT SITE: POLLUTION CONFIRMED
1. Yes 2. No 10. Other inorganics 1. Yes @No
11. Other organics
POLLUTION INCIDENT REPORTING FORM
I
Incident#---
County: £t:$),..,fj
Aasponsible Party/Names
1-1 -.. C:. -~ :r ...
Company -
~: .. --s~a-i.-. In -L
CitY .
S-1-...1-u.:, 1 .. Al,Z·
REASON FOR INCIDENT
1. Transportation Accident
., ..
RESPONSIBLE PARTY
C-..-v:,.,.
County
-r,..J ~ 11
SOURCE IN USE
0. N/A PERMIT TYPE
{) Yes
2. No O. N/A
2. Mechanical failure SOURCE PERMITTED 1. Nondlscharge
:f)=acllity design 1. Yes
,, 2. No 2. 011 terminal
4, Inventory only PERMIT NUMBER 3. Landfill
5. Human error
SOURCE ON 4. Mining
6. Vandalism ERRIS LIST
1. Yes 5. NPDES
7, Unknown ?, N~ 6. RCRA
ERRIS NUMBER
7. Air
ACTIONS TAKEN
Containment, Cleanup, etc .
.. ) .... "' 0 . ,,.,)-.... • f"lu,(,f_L•., _j~.t"JM
J
J
Nearest Populated Buildings--Type and Distance
IJ-c,c:,' MoL·1_ .1-.I .• -~
.Precipltion/Weather Data
Street Address
Rl-. I <L n ...
State
,J.C..
OWNERSHIP
0, N/A
1. Municipal
2. Military
3. Unknown
{P Private
5. Federal
6. County
7. State
I Telephone
'7o'iifl'7.3-~? !i4
"3 >0
Zip Code
Z.l?-(,"?"l
OPERATION TYPE
0. N/A
1. Public Service
2. Agricultural
3. Other Source
4. Educational
,Wl'ndustrlal
@commercial
7. Mining
Incident # __ _
CountyMtU/J/
Street Addu1ss, Road
<:'f, ,-,33
Date Incident Occurred
POLLUTION INCIDENT 'REPORTING FORM
LOCATION OF INCIDENT
l Time Incident Occurred 1
I City/Town
MnuTM,,,_)
7 112 Quad Name
Draw Sketch of Area
To I-'io
I
I
c::::Jx M·o-t·~
Lat. : Deg: Min: Sec:
Long. : Deg: Min: Sec:
0 ),/ M+-l(J.
ATTACH PHOTOCOPY OF MAP SHOWING: 1. Pollutant Source 2. Threatened Weter Supplies
3, Direction of Overland Flow
POLLUTION INCIDENT REPORTING FORM Incident # ___ _
County: lib+,dj
SOIL TYPES
COASTAL PLAIN REGION PIEDMONT SOIL REGION LANDFORM
1. River/coastal terrace 1. Middle Coastal Plain 10. Falsie Crystalline
2. Coastal (flat) plain 2. Upper Coastal Plain/Piedmont 11. Carolina Slate Belt
3. Mountain range
3. Sandhills 12. Triassic Basin
4. Sandhills 4, Lower Coastal/Wicomico, Talbot ,'@) Mixed Fe/sic and Mafic
5. Swamp 5. Lower Coastal Plain/Pamlico (5:1Linear (valley) MOUNTAIN SOIL REGION slope
6. Organic Soil
7. Brackish and Freshwater Marsh 14. 7. Head slope (concave)
Low and Intermediate Mountain
8. Nose slope (convex) 8, Outer Banks 15. Basins/Terraces/FI ood Plain
9. Large River Valleys/Flood Plain 16. High Mountain
9. Foot slope
10. Barrier island
OBSERVED AVERAGE GRADIENTS ESTIMATED DEPTHS 11. Barrier system
To nearest water supply: I % 12. Beach ridge
To uppermost confining bed:~ ft.
Water table gradient: ;J... % To water table: .h:::...h... ft. 13. Tidal marsh
To nearest stream: 2 % To bedrock:~ ft. 14. Floodplain
.l.. 15. Upland: 0-5% slope Stream gradient: % (lnterstream divide)
ESTIMATE HYDRAULIC CONDUCTIVITIES AQUIFER USE
1. LI ttl e or no use Soll Unsaturated zone Water Table Upper confined aquifer
~oderate uses 1. high 1. high 1. high 1. high
(!) medium @ medium @medium @medium
3. He a Vil y used
3. low 3. low 3. low 3. low
4. unknown 4, unknown 4. unknown 4. unknown
DISTANCE TO NEAREST WATER SUPPLY: J/ UD f 1. I DISTANCE TO NEAREST BUILDING: z:QCJ f 1.
Describe general lithology of soil and unsaturated zone
5;1, ,. 1 .... 1..; '., c~--1 :Z::../~11 c. ....... .,te. , 0~ 1:4, .5 ',J e,,,_ .... S:e:: of Ink ... , :s .,,f. ".,
,,.I, J',f(»•'I ,} s,,r t lP2 t&,.... .
Art4+e: 4z /.,, ,. ,&. .... ., fl'. -1: s-.z , ,r &» ~·.s '
c..-v<--. ._,LC/.'< w:l:J. w, ✓-·-$ .o,. ---• £.. ·//, 5!i.O l!.-t1-.._ fi;_v,.,., .r.S-J c;c,.<:,.,,,v" IS ,, ' -to I,!. zO-L/o t. ,t.. ,fl~ .4 '-'-h-./...//, e.. £;,,,,_,t:.,,,/ ,.,t. ':J ~ t.~J-.
; Provide map showing: 1. Pollutant source 2. Threatened water supplies 3. Direction of overland flow
Incident "'1 ___ _
County: ____ _
POLLUTION INCIDENT 8EPOf.lTING FORM
EMERGENCY INCIDENT RESPONSIBILITIES
RESPONSIBILITY: _____ Local ------State _____ Federal _____ Responsible party
ON-SCENE COORDINATOR:
name phone number
agency/EOG location EOG phone
EOG contacts
Assumed, date: _______ time: Relinquished, date: _______ time: ____ _
On-site representatives: -----------------------------------
TECHIICAL COORDINATOR: _______________________ _
name phone number
agency/EOG location EOG phone
EOG contacts
Assumed, date: _______ time: ______ Relinquished, date: ______ _ time: ____ _
On-site representatives: -----------------------------------
RESOURCE TRUSTEE:
name phone number
agency/EOG location EOG phone
EOG contacts
Assumed, date: ______ _ time: _____ _ Relinquished, date: ______ _ time:
On-site representatives:
PIO:
name agency phone number
Assumed,date: ________ time: Relinquished, date: _____ _ time: ____ _
'.
i
NOTIFICATIONS * 24 Hour Telephone Number
Date Agency
Spill Response Center-DEM
Water Supply-DHR
Solid/Hazardous Waste-DHR
Regional Office
Telephone
[phone]
[phone]
[phone]
Emergency Mngt.-CC&PS [phone]
Pesticides-DOA [phone]
Inland Fisheries-WAC [phone]
Wildlife Resources Commission [800) 662-7137 *
Marine Fisheries [phone]
Radiation Protection-DHR [phone]
EPA-Atlanta (404) BB 1-4062 *
Coast Guard-Wilmington [phone]
Coast Guard-Hampton Roads [phone]
National Response Center (BOO) 424-8802 *
(your supervisor) ____ _
(PIO)
(shipper) _______ _
(carrier) _______ _
CHEMTREC (Chemical Spills Only) (BOO) 424-9300 *
N.C. Poison Center [phone] *
Explosives problems-SB! [phone] *
State Warning Point-SHP
(emergencies only)
EPA-PCB problems
[phone] *
[phone] *
[phone]
Time Contact
Date:
c~ cJ O.f/
b-l6-6'l
MEMORANDUM
Well
1)
2) ...
3) J 4) j 5)
6)
7)
8)
9)
10)
11)
12)
13)
14)
15)
16)
17)
18)
19)
20)
TOTAL
j:
TO: J{)../ e~~.,t-+/-
FROM: to~y I? l',vktp-
SUBJECT1 Proposal for Drilling Assistance Region ('1~6 Date Requesting Rig ~~.,_,,if" .. tr••l15'1P I
1) Incident N ~~.r.::i..-:!!~~=:i:,_,=~~~ Incident No. 3422. 2) Location£ ,:_. 3) Nearest C .,.,_=>'!=-""""'½--.,--:cc--;---:--County ::;y.J,.,lJ 4) Contamination l'+d:r-ie I N<>.f~c -cµ:tAS~ !\ o,'-:S
5) e Invest on TI Ve..-\·t,w ..J-.l..-.+ Ma,,,:·5;.,c,u~ \n C9i"'-f~t1:~ tl.w. ,0 !!'.P":ehn-:':+•tn J..,.,, -+a fie Ml;,,.J !,.)&S~s lee,o,n> ~ 'k> o..,c.ec ... t,...:hr k/: the c.o""+"--;e:Mlon &.as m:at::r:r--f:s1 ch: _,;ir ,,_ :r+ b:·!d. 4"':f--..:..,G:f~p., kA1ii PCC!dtd M,-.. s:6d"lf"1r w:ll b~,.1'w :6 do t:L c,.(.,.,.,, e.,._r cJ. C•1±Aoi:hhd G--w• C se;:)s
6) EstJ..mated Depth To Groundwater, Average Across Site ~o• 7) No. Of Wells ~'t~-Type 6 " 4 ,Locations (See Attached Map I Bu:,ey,_ ~ "T w; 8) Well Construction
Total Total Screen Screen Depth Casing Interval Total/ Permanent/ t (ft! (ft) (ft) Well(ft) Tem~ra~ Protection
Jo :J_o :l.9 -} C> lo T t..e, 19 a c: 4 >e/ L..1< \ C.j fihu: G:nn: ~ Z.• :Z d -!C " .,
" -}o -z-o '=''" ,.. • ,, " Jo Z:::E. Z..•--1• 0
'2::0 to I
Surface
0. H!::f $ ,, ,,
1 ~,. , .... \.'i #~~~~·CJi·'•J;;.:f;· ~i:.tt~z.,.·•·t,,,'t'.':11•. ·. ~~·\jl;'~ '',.in.·-_' -J.' tJ
~. + ... + ,., _ _, -~ ;r,M.,!~-v-< . ~~l~/t
.$'1;{·'~ .:>t''
I f\C'
,t 9) Utilities On Site (see site map for locations)
1)
2)
3)
4)
5)
6)
7)
8)
9)
10)
11)
12)
13)
14)
15)
16)
l 7)
18)
19)
20)
Well No.
Power Cable
Date Located
(Above/Below)
None-&,-.:J..,[(7
" .,
I'
Gas Lines
Date Located
'' ,,
,,
Telephone
Date Located Water/Sewer
(Above/Below) Date Located
fil" t.-,2.,'?7 Moac-&-2-E?7
,/
Other
Date Loe.
____ ii
____ \I
---) __ I
10) Source of Water ~o --L""-"~------------------
1)
2)
3)
4)
5)
6)
7)
8)
9)
10)
11) Disposal Facility,For a)water and b) soil cuttings
a) J:"",-...,\,,1\ f..,..,.._f~ L.,~J {:11
b) . ?
12) Property
Well No(s)
13) RemarJ.: s:
Owner
" ..
62uA:ll L-t,7
Lease Agreements
Attached
'•
"
Warrant
Required
No
..
:::~~
. ·:· :. ~,,.,
Mr. Perry F. Nelson, Chief
Groundwater Section
Division of Environmental Management
Post Office Box 27687
Raleigh, North Carolina 27611
Dear Sir:
,w.,,;·,_:;,1; u
:i•1:c::r,,,At. urf:(~"'
Subject: Agreement for the Use of a
Site for a Groundwater
Investigation
In consideration of the site described on Attachment I and of the terms and conditions stated in this letter, I agree to permit the use of the site for a Groundwater Investigation conducted by the Groundwater Section (GWS).
This agreement for the use of the site is subject to the following terms and conditions:
(1) While either party may terminate this agreement by giving three (3) months advanced written notice, the parties may terminate the agreement at any time by written agreement.
(2) Upon written request, the GWS will supply to the owner all information derived from the investigation.
(3) Unless otherwise agreed, the GWS shall have access to the site by the shortest feasible route to the nearest public road.
(4) All costs of construction and maintenance of sites and access shall be borne by the GWS. The GWS shall protect and prevent damage to the surrounding lands.
(5) Upon termination of this agreement, unless otherwise provided for by prior written agreement, the GWS shall remove from the site all structures placed or erected by it and shall permanently abandon all wells constructed by it.
(6) The GWS has full responsibility for the acts and ,.2!l!_issions by its personnel and/or agents in connection with the construction,
maintenance, monitoring, and/or termination of the access and site.
I understand that the activities to be carried out by the GWS under the terms of this agreement are for the primary benefit of the Section and of the State of North Carolina and any benefits accruing to the owner are incidental. The GWS is not and shall not be construed to be an agent employee or contractor of the owner under the terms of this agreement.
Sincerely,
-1V~;11e/~,~ y1
Henry H. Sigmon, Jr.
Mr. Perry F. Nelson, Chief
Groundwater Section
Division of Environmental Management
Post Office Box 27687
Raleigh, North Carolina 27611
Dear Sir:
Subject:
N. C. llEPT. OF NATURAL
HESOURCh'S AND
COMMUNITY DMVF.LOl'MENT
APR 28 1887
DIVIS!Ofl OF ENl'IROi:.'.[1/i/l rg::m~rnr
MOORES\'/LLE R't"'t:mt,l CffU:E ..
Agreement for the Use o a
Site for a Groundwater
Investigation
In consideration of the site described on Attachment I and of the
terms and conditions stated in this letter, I agree to permit the use of
the site for a Groundwater Investigation conducted by the Groundwater
Section (GWS).
This agreement for the use of the site is subject to the following terms
and conditions:
(1) While either ·party may terminate this agreement by giving three
(3) months advanced written notice, the parties may terminate the
agreement at any time by written agreement.
(2) Upon written request, the GWS will supply to the owner all
information derived from the investigation.
(3) Unless otherwise agreed, the GWS shall have access to the site
by the shortest feasible 'route to the nearest public road.
(4) All costs of construction and maintenance of sites and access
shall be borne by the GWS, The GWS shall protect and prevent
damage to the surrounding lands,
(5) Upon termination-of this agreement, unless otherwise provided for
by prior written agreement, the GWS shall remove from the site
all structures placed or erected by it and shall permanently
abandon all wells constructed by it. ,.,,,.,
(6) The GWS has full responsibility for the acts and omissions by its
personnel and/or agents in connection with the construction,
maintenance, monitoring, and/or termination of the access and site,
I understand that the activities to be carried out by the GWS under the
terms of this agreement are for the primary benefit of the Section and of the
State of North.Carolina and any benefits accruing to the owner are incidental.
The GWS is not and shall not be construed to be an agent employee or contractor
of the owner under the terms of this agreement.
Sincerely,
Mr, Wade Lambert
#~ 5 ~-----·
9 -), 3 -S/7
l
,,~~;· ~~,t ~.
;i:1'1 --::-:-1~~c :1.ic: ,.,, G\llt' :,, ..
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;(<t ,.},';fKf 1•~J ., ~~t"•:J• k;~_.:.;,,,, • \h•/' " , 1; :--0 .._,} ·'.'f#.J'? ·)·i~' \'r
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i-J: ,r. ,. ... !".: ...... '! tw~"'* ,.-;~ ... :,If~~-· !~"''"• -~iif;-• J ~ l{~. . ..... _ ~ ;1:J ....... f.J ,,._,.t_,.-~~,,-r~ 1~r
.-·-:~_)''~ 1~t :·~ ,~1~: {!{~?( ~~:~ :-~tit' t:?Ji :~~ r ;:()1 ·.--;:; ~:-~~ :rt1r~ t~~f? ,_//J ~~
.~--; '{..'.'-,,.•H.f. 5.J.. ~ ;;c,~~-~k,••.,/ ~}tSv ~:,/~1 i1-'-1""°' '~:\\':;-; ':" ,, f_ -.; .' ·, . y':'?• ,·,;.>• ~~0 '··t,:t i;,:,;:~ :1;,•:;;ji,~ ~1r, ~~•-.:.. 4 ,,51;.,,_ · i-:J~~"i: ~-<tf.\ :~~,,,_~:;,;,'..?: .. ;:,;,:'~ N-t;. ,.>• l ,,~· 1~--·, ;;t''\ :"-,; ·-~ ,'·:f.''-~?<'/ ;_';'.~[' t~~-::q •,:}'f :~}J. •T;t~ "\; (j❖t;,.'-; ~•~(;,~'(: 1ri~• ~ 4,~;;"~ ~,;. •••~• j~r ~.:f. ,\i'..Jyt ( ~•-! ,~; • , . ':.'!• <',, ,'~, ,.~~:, /~f';;
~.,\}/"•''".>,, •,, ,J;v ,•t,:, ;.•k'"c.. ',,,:.,· .,-,'!;~•;!!.rc•,,<f.ll1•, ~,,.-,tr'•.· f.:l(\1,cci'e .._; 't, ;' 1.,.•~ _.,,;.;:-,: ~'., ,.-..:cr 1·~~--1\t ~; ~,.,~--SI I;: "~t-~.C.1 .•'::ttr~1 ':•t:~ ..,~:.,.; {.,e.-',.";;..>,,;",:' \j'"•"•'''. ~-0 .• .;~~-.;;;:·,,_,,~j'· •¥ ':~\\J ,,, ~·-,~I' (<1; 1:·-: ., ~ : · :;: '~, ... ,? :,.;-; ;':io,:,)'~ ::2-;-,:;ti 7;,';...:~~-~ .;:~' ·/• -;;, J·/ ,-,.~ -:t J ' _' r ~--;-~ :··; :; \:· r.:::l.5· 1'-:f. ~t,, i,'i\•~!•lr:,' .,~·~r.•{lt>' ... , ~ ~-t.;I"')t~l•¼·XJ)j~'-.,~,~· ;• ~, ~ 1,,,,,.,1,,·,,,. -tJ-. .-1,,· ''R_'J·~~{I.-" ~tt \:.r:: ~f: ~tt ~f~J~\ ~~:;~~, ~~;;;~ t{~~ :y}~i-~~~~-i~~_(j t;/t ~:. :-· ~ .. ~ -~tt , t/:~;;;: ~:~-;12· •i
,1,.t :', l>sf""' '~~! d f~...,.,1\ f-'] ,_ -J,1\•~-,;,;..-;;~ •,.:_.'!;'jJ~ -~i'-~•1 1~.11 ~-c:~--.-., l ,;,: J ,.,, Iv '• r"~-,~~ ' -, "•r·❖•, t· ,, . .;;,1.•\l •'f.'•
,'J;. ;ri;,:.i ;:-' .. )'{ ~~~1 i11i \t•ii,! ~I·{ii: ·-~" :+'":·, ·,,,, •-:1~ ii;J: ,~}\ ,) -~-i",-.'~(f~; :f\ •;:(}; ftlt l;~t
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170 Security •·• c:c,L·e, -,YELLOW PAGES
A~A ENTERPRISES I NC
H A DIVISION OF .. .
SIGMON -SEPTIC TANK SERVICE
"HENRY H SIGMON JR -OUR FAMILY SERVING YOURS SINCE 1948"
• PUMPING SEPTIC TANKS ------' · -· · '
• MAINTENANCE CONTRACTS.AVAILABLE 'CAR WASH HEALTH DEPARTMENT APPROVED
•RESTAURANT GREASE TANKS, 'SAND BAY~ 24 HOUR SERVICE
INDUSTRIAL WASTE. DISPOSAL ·PUMPED
SEWER LINES OPENED BY VAC OR REEL RESIDENTIAL -COMMERCIAL -INDUSTRIAL
-SEPTIC TANKS INST ALL ED -
WE.LEAVE
PREMISE CLEAN
8ACKHOE
"NO JOB TOO SIIIALL
NO J08 TOO LARGE"
CUSTOM BACKHOE SERVICE
DRAIN FIELD REPAIR
LANDSCAPING
SERVING N.C. & S,C.
500FT
OF HOSE
873-8954
STATESVILLE TEL NO
HOME 528-6321 . EUFOLA RD TROUTMAN
I
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:SC.AL€ : I".: 100 ,.
r,
~ C:,'
State of North Carolina
Department of Natural Resources and Community Development
Mooresville Regional Office
James C. Martin, Governor
S. Thomas Rhodes, Secretary
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
Mr. Henry Sigmon, Jr.
Sigmon Septic Tank Service
Route 14, Box 350
Statesville, North Carolina 28677
Dear Mr. Sigmon:
Albert F. Hilton, Regional Manager
DIVISION OF ENVIRONMENTAL MANAGEMENT
March 31, 1987
The Groundwater Section of the Division of Environmental Management
is currently investigating possible groundwater contamination caused by
unlined waste pit lagoons located on your property off S. R. 1133 in Iredell
County.
In order to verify that groundwater contamination has or has not occurred,
the Groundwater Section must conduct a subsurface investigation. This
investigation would include augering several boreholes into the unconfined
aquifer.
Prior to augering at any site, the enclosed agreement must be signed
and dated and returned to the Raleigh address within two (2) weeks. Failure
to allow the Division access to the property may result in an administrative
inspection warrant being secured in order to conduct the investigation. The
diagram on Attachment I shows the proposed augering sites.
Should you have any questions concerning this agreement, please call me
at [phone].
cc: /Lee Laymon / vMr. William Jeter
Mr. Tony Parker'7''f'
~ /~~~
Ronald L. McMillan
Regional Supervisor
919 North Main St=t, P.O. Box 950, Mooresville, N.C. 28115-0950 • Telephone [phone]
An Equal Opportunity Affirmative Action Employer
.,.
Attachment I
The site which is the subject of this agreement is located .03 mile northwest of Buffalo Shoals Road (S. R. 1004) and the junction of Eufola Road (S. R. 1333) in Iredell County.
C
l. ' . • --

.

-6.t .. -. • ·;.-.i-:;1 .
~.r.,.( . ··'".•-"; ·~ <:.... .
' i ' ·: I • j.
l 4 ~ < ' ~-:~---.,,,,
,.
T . ' e
t
j -
u..:•• •• u..ll,.a4
-~._ L..~••~S
•' •
i)!!_;:l/i:
Mr. Perry F. Nelson, Chief
Groundwater Section
Division of Environmental Management
Post Office Box 27687
Raleigh, North Carolina 27611
Dear Sir:
Subject: Agreement for the Use of a
Site for a Groundwater
Investigation
In consideration of the site described on Attachment I and of the terms and conditions stated in this letter, I agr.ee to permit the use of the site for a Groundwater Investigation conducted by the Groundwater Section (GWS).
This agreement for the use of the site is subject to the following terms and conditions:
(1) While either party may terminate this agreement by giving three (3) months advanced written notice, the parties may terminate the agreement at any time by written agreement.
(2) Upon written request, the GWS will supply to the owner all information derived from the investigation.
(3) Unless otherwise agreed, the GWS shall have access to the site by the shortest feasible route to the nearest public road.
(4) All costs of construction and maintenance of sites and access shall be borne by the GWS. The GWS shall protect and prevent damage to the surrounding lands.
(5) Upon termination of this agreement, unless otherwise provided for by prior written agreement, the GWS shall remove from the site all structures placed or erected by it and shall permanently abandon all wells constructed by it.
(6) The GWS has full responsibility for the acts and omissions by its personnel and/or agents in connection with the construction, maintenance, monitoring, and/or termination of the access and site.
I understand that the activities to be carried out by the GWS under the terms of this agreement are for the primary benefit of the Section and of the State of North Carolina and any benefits accruing to the owner are incidental. The GWS is not and shall not be construed to be an agent employee or contractor of the owner under the terms of this agreement.
Sincerely,
Henry H. Sigmon, Jr.
1
2
J
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
A
B
C
i
COUN II ::z;;; «J , J I
RIVER BASIN: ere,
REPORT TO: ARO. F~O.~ RRO. WoRO WiRO WSRO TS
Othe, 8,\k I<. U"s I S--M ,(()
Sh;pped by B"!80t~e,
COLLECTQR{Sl· ~
BOD RANGE' SEED'
0 It u I 3 !, ➔ J " J L 0'1J: f? a £3' 0 7
. , ; "'::tf ("\"
N .C :--EPT. :oF NATURAL RESOURCEJi.-A.~•···-Jf.ilTY
DEVELOPMENT ' \)\J
DIVISION OF: ENVIRO~Mt~L ~lNAGEMENT
WATER QUALITY ~00 FORM (OMll G t SAMPlE TYPE ' □EMERGENCY □SPLIT ~MPLIANCE □AMBIENT
STATION 1ocA110NG:en<. S;~,..,en
REMARk'C:.:
3 . 4 . 2 7 Vim• o/ :wa_,.-,.
-:;-the,
DATA ENTRY
DATE REPORTED·
Slotion Number Dole 8111gin1 yy/mm/uu! Time Begin Dote End Time End Depth DM DB DBM Volue Type Compo\ire Sample Type
0-. s .. \, L,__j
BOO" 1.1n
COO Hi<>h 140
CO0·Low JJS
Colilo,m:MF Fe(ol 31"1"
Colilo,,....,MF Torot """4
Coliform. Tube Fe col 3lAJ5
Coliform Tube Total "'1"05
R•sidue· Total· --
Va101ile 5n5
fiud <..lQ
Ruidue:<-----nded <,3Q
Volorilt-535
f:,ed c,,40
-H ◄n3
Acidir,.. to aH 4 5 4]b
A1i2!.!.] 1ao~i8) '"
Al~~ti,,ih, 10 ... u B.) 415
Alf,oliriilt 'S! eH 4 S 410
,oc • D"
Jvibidi,,, 7A
SomplinQ Poin1 Wote, lempero!ure("C)
Pl 1; .,
Secchi (Mele<\)
" I Hr Senleo~le Mottet (ml/lfHr.1
50086
OM l/lf•,,,ud
7-85
,o
Air Tempe,otur• ( 'C)
2D
Oeod f i,h Severity
1340
! lx1 103 10:} }loo! I
mo/I Chlo,ide94n 1
mo/I v· Anenic: Tolnl ,,,.,.,.;
ma/ Chi a: ,., 32217 I
/J00ml Chi o ·Corr ...,..,20Q
!
1100ml Ph,.onhulin O 32213
I
1100ml Color: True RO '
I
/I00mll Chromium:He• 1032
mn/f Cvonidc 770 i
mo/I Flu"•ide9<..l !
mo/j Formoldehude 71880
mn/1 Greou and Oil1 556
mn/j Hordness:Jatol 9"~
mo/I MBAS 38760 I
unih Phenols 32730 !
mn/1 Sulfole 945 I
mn/1 Sulfide 745 I
m<>/1 Soecilic Cond. 95 I
I mo/I Biomou= Dru Wt. S73
mo/I Biomou: Peri Ash iF,ee 577.
NIU Chi o: Peri fluro ;825-17
I ! o.o. pH
I ,l I. JD0 4D0
0.0. '\ Sotu,olion Salinity 't. ; ,
JOI 480 ;
Turbiditr Se,,erily Qdor:Almo,phere
Severity l 1350 1330
A H l r s B C G GNXX
I
mo/I NH> a, N 610 mo/I X' Ni -Nici.el 1067 ~.so ug/1
::?~ uo/1 TKN as N 675 mo/I X P'--'eod 1051 60 ua/1
11n/l NO.., •NO., o, N 630 mo/I Sb Antimnn" 1097 uo/1
ua/1 PO· as P 70507 ma/I Se Seleni··m 114.., ua/l
un/1 p J01ai O\ P 665 mn/l V' Zn Zinc 109.., ..2:300 va/1
P1-Co p, Diuolved OS p 666 mo/I
uo/1 y A" Silver 1077 ~,;i5 uo/1 Pesticides S -cilicoll
mn/1 )( /4, oou un/1 :; , )-
Al -Aluminum 1105 ' -., ScCln Or9onochlorine
.
mo/I Be..:. Ber.,ltium 1017 m/1
mo/I Co -Calcium 916 mo/I , --$con~Orna"".-.h.,...._,...hJ
mn/J ~-<;D f-::;..1,1, ..:-l -, 1 \:10 I
Cd -Cadmium 102 7 oat
m"/1 Ca Cobalt 1037 uo/ I y £il~dn\~~·-:~:e~i;·;c~fr: \ .:-:: :_~ itJ rt
mo/I ){ Ch,omium T-101 1034 <,;z5 l\t\~ ~::_•,1~1 I,. ,.
uo/1
u<>/1
.,.
Cu-Co t-r 1047 ~5D ua/ I )' Scan Bose / Neutral Ex1rm1able1
ma/I )( Fe-Iron 1045 II ,....., D uo/ l ),' Scan Acid b:.1roctobles
mo/I 'X H----Mercur., -D O,& uo/ I .... ~'-?
' _ rV.,
uMhos/(m Li --Lithium 1137 UQ/ I Soeciol Anolvsis i · ---
' ~ Mn -Monne,ium 97 7 -:z, 1 ,<;) 'J ,~\J-
9/M, ...... !!!2.D
' ')f Mn-Monoanese 1055 _:::/5'D c • ~~q"'~ b:·rbicides 8/M ~
' y .;l ;:::; =--' mQ/M Na Sodium 979 mo/I ,G. i-~~r~eobles
-,;;v \"
Conductance Alkalinity Acidity
al 7S"C PH 8.3 pH 4 .S PH4.5 PH 8 . .1
94 82744 4JT 87743 87247
Algoe,Flooting Mot, Pr ec i p1 tol ion (In/Doy) Cloud Covt-r. ' Se ... erity
Wind Di1ection{0eg I Wind force
Beovlort
1325 45 " Jb J7
5treom Flo""' Detergent Sud, Oil-Grll'O\e Flooling Debris ~ludge Se,,erily S:.:ve,ity Se,..erily Se,,erit) Severity
1351 1305 1300 1)4 5 l31~
' '
Reported by [Y.lJ
J
Date ,fl/ :;i_ 't / 'l f I , I
Checked by r A ORGANIC ANALYSIS
Entered b~
Checked by T::;f-
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Lab No. Sample Tvoe: h1,:z-fev Analytical Results
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