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HomeMy WebLinkAboutNCD003446721_20050627_Celeanse Corporation - Shelby Fiber_FRBCERCLA RA_OU-1 Semiannual Report January - June 2005-OCRI I I I I I I I I I I I I I I I I I I Post Office Box 2732 IO Tampa, FL 33688-32IO 8 I 3-265-2338 FAX-265-3649 Mr. Kenneth A. Lucas U.S. EPA Region IV Atlanta Federal Center 6 I Forsyth Street Atlanta, GA 30303-8960 Kubal-Furr & Associates Environmental Management Services July 27, 2005 Re: OU-I Semiannual Report-Ticona, Shelby-January 2005-June 2005 Dear Ken: Post Office Box 80247 Simpsonville, SC 29680-0247 864-962-9490 FAX-962-5309 On behalf of CNA Holdings, Inc., we are pleased to enclose two copies of the report entitled: "Operable Unit I-Semiannual Report-January 2005-June 2005-CNA Holdings, lnc.-Shelby, North Carolina." By way of this letter, we have also transmitted a copy of the report to David Mattison with NCDENR for his review. Please contact me at 813-265-2338, to discuss any questions you may have following your review of this document. Sincerely, Kubal-Furr & Associates Jz/{;__~- Jerry E'. Kubal, P.G. President cc: David Mattison, DENR Rick Ramirez, Celanese Americas PEM Carter, Ticona Kubal-Furr & Associates ----------- I I I I I I I I I I I I I I I I I I I CNA Holdings, lnc./Ticona-Shelby, NC-Ql IQ2 2005 Semiannual Report I Page i Contents Page Acronyms/ Abbreviations ............................................................................................................................ .iii 1.0 Introduction .......................................................................................................................................... I 2.0 Work Performed ................................................................................................................................... 3 2.1 1st Quarter 2005 ........................................................................................................................... 3 2.2 2nd Quarter 2005 ......................................................................................................................... 4 2.3 Free Product DowTherm®A Bailing-Well F-55 .................................................................... 4 3.0 Discussion of Findings ......................................................................................................................... 5 3.1 Ground-Water Movement ........................................................................................................... 5 3.2 Ground-Water Quality ................................................................................................................. 5 3.3 Discussion of Analytical Test Results ........................................................................................ 6 4.0 Review of Selected Historical Water-Quality Data ........................................................................... 8 5.0 Closing Comments .............................................................................................................................. IO Tables Table I. 2005 Sampling Matrix-CNA Holdings, Inc.-Shelby, NC Table 2. Summary of Selected CERCLA-Related Water-Quality Data-(lst Quarter 2005) Table 3. Summary of Selected CERCLA-Related Water-Quality Data-(2nd Quarter 2005) Table 4. Summary of Selected PEW-Related Water-Quality Data-( I st Quarter 2005) Figures Figure I. Site Location Map-CNA Holdings, Inc./Ticona-Shelby, NC Figure 2. Potentiometric Surface Map-Shallow Saprolite-February 10, 2005 Figure 3. Potentiometric Surface Map-Deep Saprolite/Upper Bedrock-February 10, 2005 ------------Kubal-Furr & Associates ------------ n I I I I I I I I I I I I I I I I I I I CNA Holdings, lnc./Ticona-Shelby, NC-QJ/Q2 2005 Semiannual Report I Page ii Figure 4. Hydrogeologic Cross Section-February IO, 2005 Figure 5. Potentiometric Surface Map-Shallow Saprolite-May 2, 2005 Figure 6. Potentiometric Surface Map-Deep Saprolite/Upper Bedrock-May 2, 2005 Figure 7. Hydrogeologic Cross Section-May 2, 2005 Attachments Attachment 1. Analytical Data Package, Data Assessment Summary and Field Sampling Logs for the !st and 2nd Quarter 2005 Sampling Events Attachment 2. Selected Water-Quality Plots Attachment 3. Back Cover-CD ROM of Semiannual Report in pdf Format ------------Kubal-Furr & Associates ------------ I I I I I I I I I I I I I I I I I I I CERCLA CFO CNA DENR EPA ESD Fil FP GC/FID !MAC ITC! ITEF LTRA MCL MEK mg/L MNA NFG NPL OTC! OTEF OU-I OU-2 PCE PEW ROD SBR svoc TCE TCLP TOC voe CNA Holdings, Inc./Ticona-Shelby, NC-Ql/Q2 2005 Semiannual Report I Page iii Acronyms/Abbreviations Comprehensive Environmental Response and Liability Act Celanese Fiber Operations CNA Holdings, Inc. (North Carolina) Department of Environment and Natural Resources U.S. Environmental Protection Agency Explanation of Significant Differences Fiber Industries, Inc. Filter Press Gas Chromatograph/Flame Ionization Detector Interim Maximum Allowable Concentration (North Carolina) Inner Tier Combined Influent Inner Tier Effluent Long Term Remedial Action Maximum Contaminant Level Methyl Ethyl Ketone (2-Butanone) Milligrams per Liter Monitored Natural Attenuation National Functional Guidelines (for organic/inorganic data review) National Priorities List Outer Tier Combined Influent Outer Tier Effluent Operable Unit I Operable Unit 2 Tetrachloroethene Polymer Extraction Well Record of Decision Sequencing Batch Reactor Semivolatile Organic Compound Trichloroethene Toxicity Characteristic Leaching Procedure Total Organic Carbon Volatile Organic Compound ------------Kubal-Furr & Associates ------------ I I I I I I I I I I I I I I I I I I I CNA Holdings, lnc.!Ticona-Shelby, NC-Ql/Q2 2005 Semiannual Report I Page I 1.0 Introduction Ticona, an operating subsidiary of Celanese, owns and operates a polyester and engineering plastics production facility in Shelby, North Carolina. CNA Holdings, Inc. (CNA), also a subsidiary of Celanese, retains management of environmental matters for the corporation and thus, is responsible for the work performed during the semiannual reporting period. The Shelby site consists of an approximate 450-acre piece of property which includes the main plant production area, wastewater treatment area, former waste disposal areas, and recreational areas. The plant is located in south central Cleveland County, bordered by NC Highway 198 to the west and Lavender Road to the south, approximately one mile north of Earl and six miles south of Shelby. A site plan showing the location of production areas, monitor wells, extraction wells, and other significant features is shown on Figure I. Operations at the site began in 1960 by Fiber Industries, Inc. (Fil), a manufacturer of polyester chips and filament yarn. Celanese Corporation bought the facility from Fil in 1983, renaming it Celanese Fiber Operations (CFO), and continued the production and processing of polyester polymer chips and fibers. The site has alternately been known as HNA Holdings, Inc., Hoechst Celanese Corporation, and Celanese Fiber Operations, the latter being the site name as listed on the National Priorities List (NPL). CNA currently maintains a long term remedial action (L TRA) system at the CFO site, designated as Operable Unit I (OU-I) in the Record of Decision (ROD). OU-I consists of two ground-water extraction and treatment systems identified as the Inner Tier and Outer Tier systems. OU-I became operational in August of 1989. A second operable unit, OU-2, consisted of excavation, incineration and reburial of stabilized incinerator ash and other inert waste materials. Current status of the OU-I LTRA is discussed below. On April 21, 1998, OU-2 and the Outer Tier portion of OU-I were shut down as part of a partial delisting petition approved by the EPA effective April 17, 1998. Further, implementing EPA recommendations in the August 200 I Five-Year Review Report, the Inner Tier was shut down on March I, 2004 while CNA implements and evaluates an MNA (monitored natural attenuation) demonstration project. ·· The entire Outer Tier is being maintained in "standby status" as part of the delisting process and can be brought on-line within a relatively short period of time if it is found necessary to provide hydraulic control along the property boundary. The Outer Tier wells functionality is assured by performing routine monthly and quarterly system checks such as energizing the well pumps, transfer pumps and blowers, -------------Kubal-Furr & Associates ------------- I I I I I I I I I I I I I I I I I I I CNA Holdings, Inc./Ticona-Shelby, NC-QJ!Q2 2005 Semiannual Report I Page 2 verifying heater operation, etc. and performing maintenance activities as required by the routine system checks. With an effective date of April 23, 2004, an ESD (Explanation of Significant Differences) was utilized to modify selected elements of the remedial alternatives contained in the OU-I ROD. The ESD provides for CNA to discontinue treatment of recovered ground water in a separate ground-water treatment system (consisting of a sequencing batch reactor [SBR], air stripping and carbon polishing) and instead to reroute recovered ground water to the existing industrial wastewater treatment plant. This modification is scheduled to take place following review of the outcome of the MNA demonstration project at which time a decision will be made as to the need to restart the Inner Tier recovery well system. Currently, CERCLA-related (Comprehensive Environmental Response and Liability Act) LTRA monitoring activities consist of quarterly sampling of selected monitor wells (Table I) and submittal of semiannual reports to the EPA (Environmental Protection Agency) and DENR (State of North Carolina Department of Environment and Natural Resources). Non-CERCLA semiannual sampling of PEW wells (polymer extraction wells) also takes place and these data are submitted along with the routine semiannual CERCLA reports. Samples are also collected quarterly from selected monitor and extraction wells as part of the MNA demonstration project and are reported separately to the agencies in the form of quarterly data collection reports. Kubal-Furr & Associates (Kubal-Furr) has prepared this semiannual OU-I operating summary report for submittal to the EPA and DENR on behalf of CNA. It covers the period from January I, 2005 through June 30, 2005 and includes the results of analytical testing of samples collected during the periods February 15-23, 2005 and May 4, 2005. ------------Kubal-Furr & Associates ------------ I I I I I I I I I I I I I I I I I I I CNA Holdings, Inc./Ticona-Shelby, NC-QJIQ2 2005 Semiannual Report I Page 3 2.0 Work Performed As part of the OU-I remedy, CERCLA-related samples are collected at selected monitor wells and analyzed for the parameters summarized in Table I. In addition, samples are collected from the inactive PEW system and selected PEW-related monitor wells. The location of all monitor and extraction wells is shown on Figure I. A description of the work performed during this reporting period is provided below. 2.1 1st Quarter 2005 On February IO, 2005, water levels were measured by Kubal-Furr in a total of I 16 monitor wells, extraction wells, and piezometers. A total of 13 CERCLA-related ground-water quality samples were collected during the period February 15-23, 2005, in accordance with the sampling matrix shown in Table I. All samples were collected by Kubal-Furr and analyzed by Davis & Floyd Laboratories of Greenwood, South Carolina. OU-1 Monitor Well Sampling Thirteen monitor well samples were collected using low-flow sampling protocols. The samples were analyzed in the field for pH, temperature, conductance, turbidity, dissolved oxygen (DO) and oxidation reduction potential (ORP); and, by the laboratory for volatile organic compounds (VOCs) using EPA Method 82608. In addition to analysis of volatiles, samples from monitor wells V-23 and K-28 were analyzed by the laboratory for total organic carbon (TOC) using EPA Method 9060. PEW Extraction and Monitor Well Sampling Three PEW grab samples (PEW-I, PEW-3, and PEW-4) and one monitor well sample (F-55) were collected during the I st Quarter. These samples were analyzed in the field for pH, temperature, conductance, turbidity, DO and ORP; and, in the laboratory for VOCs by EPA Method 82608 and for SVOCs (semivolatile organic compounds) by EPA Method 8270C (including the DowTherm®A constituents I, 1-biphenyl and bi phenyl ether). -------------Kubal-Furr & Associates ------------- I I I I I I I I I I I I I I I I I I I CNA Holdings, lnc.!Ticona-Shelby, NC-Ql!Q2 2005 Semiannual Report I Page 4 2.2 2nd Quarter 2005 On May 2, 2005, water levels were measured by Kubal-Furr in a total of I 16 monitor wells, extraction wells, and piezometers. Water-quality samples were collected from two monitor wells (V-23 and K-28) and were collected on May 4. 2005 by Kubal-Furr and analyzed by Davis & Floyd. These wells were analyzed in the field for pH, temperature, conductance, turbidity, DO and ORP; and, by the laboratory for TOC by Method 9060. 2.3 Free Product DowTherm®A Bailing-Well F-55 As discussed in earlier semiannual reports, free product DowTherm®A was found to be accumulating in monitor well F-55 following a monitor well rehabilitation program implemented in September 200 I. Prior to the current semiannual reporting period, well F-55 was sounded/bailed on 15 separate occasions since March of 2002 and the total volume of DowTherm®A recovered was approximately 2.43 gallons (9.19 liters). Well F-55 was bailed during the 1st and 2nd Quarters and 0.23 gallons (0.88 liters) of free product was recovered (0.13 gallons [0.49 liters] and 0.10 gallons [0.39 liters] in the I st and 2nd Quarters, respectively), bringing to 2.66 gallons (10.07 liters) the total amount of DowTherm®A recovered to date. This well will be tested again in the 3rd and 4th Quarters of 2005 and any free product accumulations will be removed and recorded. ------------Kubal-Furr & Associates ------------ I I I I I I I I I I I I I I I I I I I CNA Holdings, lnc.!Ticona-Shelby, NC-Ql/Q2 2005 Semiannual Report I Page 5 3.0 Discussion of Findings 3.1 Ground-Water Movement As previously discussed. water levels were collected on February 10, 2005 by Kubal-Furr, and again on May 2, 2005. These data were used to construct potentiometric surface maps and hydrogeologic cross sections (Figures 2 thru 7). The shallow saprolite maps (Figures 2 and 5) show water-level contours and direction of ground water movement in the uppermost water-bearing zone beneath the site. The direction of movement in this zone is to the east, northeast and southeast from upgradient areas along NC 198, towards discharge areas along the unnamed tributaries of Buffalo Creek. An attempt was made to separate the uppermost water-bearing zone from the deeper saprolite and upper bedrock zone. While these maps (Figures 3 and 6) present a reasonable picture of ground-water movement in this zone, it should be pointed out that it is giving a more generalized picture of ground- water movement because of the well construction techniques used in many of the wells and piezometers. The typical construction of these wells was to have relatively long screens and extremely long sand packs in the annular space above the screens. As a result, the lower saprolite/upper bedrock maps have a number of composite head values measured along a longer screened area. However, the maps may be useful for determining the general direction of ground water movement. Hydrogeologic cross sections were also constructed from the February and May data sets (Figures 4 and 7). The location of the cross section is shown on the site location map, Figure I. The east-west cross section (A-A') is constructed through the plant and indicates flow is predominantly horizontal across the site, from up gradient areas west of the plant toward downgradient areas to the east. 3.2 Ground-Water Quality The analytical data for the I st and 2nd Quarters of 2005 were evaluated using method specific quality control criteria and, for additional guidance when necessary, the EPA's National Functional Guidelines (NFG) for organic and inorganic data review. ------------Kubal-Furr & Associates ------------- I I I I I I I I I I I I I I I I I I I CNA Holdings, lnc.!Ticona-Shelby, NC-Ql/Q2 2005 Semiannual Report I Page 6 The I st and 2nd Quarter data were considered quantitative with several exceptions as noted in the Data Assessment Summaries (Attachment I). Based on the data-quality assessment, qualifiers were. placed on selected analytical results as noted in Tables 2 and 4. Acetone was detected in the field blank collected on 2/22/05 at a concentration of 0.016 mg/L. Consequently. the acetone for sample P-58 was flagged with a "U" qualifier as non-detect. The phenol result for field sample F-55 was flagged with a "J" qualifier as estimated, due to low recovery of surrogate and recovery values for phenol in the associated matrix spike/matrix spike duplicate samples that exceeded control limits. Benzene, methylene chloride and toluene results from well F-55 were assigned an "X" qualifier by the laboratory to indicate a higher reporting limit due--}matrix interference. The X qualifier had no affect on..latl1iusability . .(J-._ 3.3 Discussion of Analytical Test Results Analytical test results, field sampling logs, and chain-of-custody forms for the I st and 2nd Quarter data sets are contained in Attachment I. A summary of selected analytical data for the I st and 2nd Quarters is presented in Tables 2, 3 and 4. CERCLA-Monitor Wells Of the 13 CERCLA-monitor well samples analyzed during the reporting period, 6 had volatile organics reported above the detection level (Table 2). Of these six, three (V-23, CC-33, and K-28) had two or more individual volatile constituents reported as present above the detection level. The most frequently reported volatiles included trichloroethene (TCE) (three detects), and benzene and toluene (at two detects each). Monitor wells V-23 and K-28 reported the largest number of individual volatiles at four each. V-23 reportedly contained benzene (0.021 mg/L), ethylbenzene (0.003 I mg/L), toluene (0.0 IO mg/L), and total xylenes (0.012 mg/L). K-28 reportedly contained 2-butanone (MEK) (0.084 mg/L), acetone (0.12 mg/L), benzene (0.0083 mg/L), and toluene (0.0020 mg/L). CC-33 reportedly contained two volatiles (chlorobenzene at 0.0019 mg/L, and cis-1,2-dichloroethene at 0.0022 mg/L). T-35, HH-48 and HH-77 reported the presence of one volatile, TCE, at 0.0016 mg/L, 0.20 mg/L, and 0.38 mg/L, respectively. Benzene and TCE were the only constituents reported above a North Carolina 2L ground-water quality standard (two instances each). ------------Kubal-Furr & Associates ------------ I I I I I I I I I I I I I I I I I I I CNA Holdings, Inc.!Ticona-Shelby, NC-QJ/Q2 2005 Semiannual Report I Page 7 Monitor wells K-28 and V-23 were also analyzed for TOC during the 1st and 2nd Quarters. K-28 was reported to contain 60.4 mg/L and 52.7 mg/L TOC during the I st and 2nd Quarters, respectively. V-23. was reported to contain 10,700 mg/Land 8,900 mg/L TOC during the 1st and 2nd Quarters, respectively. PEW-Related Samples Four PEW-related samples were collected during the I st Quarter. No volatiles were reported as present in the sample from PEW-3. PEW-I reportedly contained the volatiles cis-1,2-dichloroethene (0.0012 mg/L), chloroform (0.0016 mg/L) and trichloroethene (0.0055 mg/L). PEW-4 reportedly contained the volatiles benzene (0.0026 mg/L), cis-1.2-dichloroethene (0.0056 mg/L) and trichloroethene (0.015 mg/L). F-55 was reported to contain the volatiles benzene (0.051 mg/L), methylene chloride (0.014 mg/L), and toluene (0.0057 mg/L). Three of the four PEW-related samples (F-55, PEW-3 and PEW-4) had reportable quantities of DowTherm®A constituents (i.e., 1,1-biphenyl or biphenyl ether). I, 1-Biphenyl was reported as present in well F-55 (20.8 mg/L) and PEW 3 (0.27 mg/L). Biphenyl ether was reported as present in F-55 (62.7 mg/L), PEW-3 (0.86 mg/L) and PEW-4 (0.026 mg/L). Benzene, methylene chloride, TCE, 1, I bi phenyl and 2-methylnaphthalene were the constituents reported above a North Carolina 2L ground-water quality standard. Well F-55 reportedly contained the largest number of constituents at seven, and the largest number above a 2L standard at four (benzene, methylene chloride, I ,I biphenyl and 2-methylnaphthalene). PEW-4 reportedly contained four constituents, two above a 2L standard (benzene and TCE). PEW-I reportedly contained three constituents, with one above a 2L standard (TCE). PEW-3 reportedly contained two constituents, with none exceeding a 2L standard. -------------Kubal-Furr & Associates ------------- I I I I I I I I I I I I I I I I I I I CNA Holdings, Inc.!Ticona-Shelby, NC-QJ/Q2 2005 Semiannual Report I Page 8 4.0 Review of Selected Historical Water-Quality Data Attachment 2 contains plots of water-quality constituents for selected monitor wells. The choice of locations and constituents was based on a review of the water-quality database, in particular those locations having any meaningful data to plot. In general, only those monitoring locations within a few hundred feet of the former OU-2 source area have any significant number of water-quality constituents reported above the detection limits. In order to assess long-term trends and improvement in water-quality conditions resulting from source removal and prior ground-water recovery, the following locations and constituents were selected for review: • Monitor Well Y-23 TOC, 2-butanone (MEK-methyl ethyl ketone), acetone and benzene data. The V-23 TOC concentrations began trending downward from a high of 8,000 mg/Lin mid-1989 to less than 1,000 mg/L in early 1992. Since that time, the TOC data have shown several wide swings in concentration, with it not being uncommon to note quarter-to-quarter changes of more than 4,000 mg/L. Since 1996, the TOC values have generally fluctuated in the range of 3,000 mg/L to over 12,000 mg/L, although the most recent 2nd Quarter 2005 value of 8,900 mg/L represents the lowest TOC reported in the previous seven quarters. The V-23 MEK data have generally fluctuated in a narrow range below I mg/L, and the last 16 sample results have all been reported below 0.5 mg/L, with the last 5 quarterly samples reported below detect. The V-23 acetone test results had generally been oscillating between 0.2 mg/Land 0.5 mg/L for the past four years, however, the last four quarterly samples have been reported below the detection level of 0.0050 mg/L. While more than half the benzene data for Y-23 are flagged as estimated or below the detection limit, 18 of the past 22 sampling events have been quantitative and show benzene to be fluctuating in a narrow range of from 0.01 to 0.03 mg/L. • Monitor well K-28 TOC and benzene data. TOC and benzene have both shown a steady decrease in concentration beginning about the time the OU-2 source remediation began in January of 1991. The TOC concentrations at K-28 have shown several wide swings in concentration up to 2,710 mg/L during the past three years and these increases may be related to a combination of a well rehabilitation program undertaken in 2001 and shutting down the Inner Tier extraction wells. The most recent two ------------Kubal-Furr & Associates ------------ I I I I I I I I I I I I I I I I I I I CNA Holdings, lnc./Ticona-Shelby, NC-QJIQ2 2005 Semiannual Report I Page 9 quarters (I st and 2nd Quarter 2005) were reportedly back down to pre-200 I levels (at 60.4 mg/L and 52.7 mg/L, respectively). Although benzene had also shown a general decline since OU-2 source remediation, the concentrations had increased since the 2nd Quarter of 2003 from 0.0057 mg/L to 0.0 I I mg/L during the I st Quarter of 2004. The most recent sample for benzene at K-28 (I st Quarter of 2005) was reportedly back down to 0.0083 mg/L. • Monitor well HH-48 and HH-77 TCE data. The HH-48 TCE test results had shown a decline from 0.222 mg/L in August of 1995 to less than 0.1 mg/L during the 3rd Quarter of 2000. Since that time, TCE concentrations at HH-48 had steadily increased to a 3rd Quarter 2003 value of 0. I 9 mg/L. TCE receded between the 3rd Quarter 2003 and I st Quarter 2004 but was noted to increase again between the I st and 3rd Quarters of 2004 and the I st Quarter of 2005. TCE at HH-77 had been trending upward between 1989 and 1996 when it peaked during July 1996 at 0.383 mg/L. TCE at HH-77 subsequently decreased substantially to 0.059 mg/L during the I st Quarter of 200 I, however, the concentration was noted to increase during the 3rd Quarter of 200 I (0.35 mg/L) and to achieve a high of 0.46 mg/L during the 3rd Quarter of 2002. The 3rd Quarter 2003 concentration of TCE at HH-77 had reportedly receded to less than 0.05 mg/L, its lowest level since 1990, but during the I st Quarter 2004, the concentration rose again to 0.31 mg/L and during the 3rd Quarter 2004 achieved a historic high of 0.47 mg/L. The TCE at HH-77 has since receded to 0.38 mg/L ( I st Quarter of 2005). The presence of TCE at these locations (HH-48 and HH-77) are thought to be the result of a localized source on the former Elliott property, unrelated to activities at CNA/Ticona or the former OU-2 source area. ------------Kubal-Furr & Associates ------------ I I I I I I I I I I I I I I I I I I I CNA Holdings, Inc./Ticona-Shelby, NC-QIIQ2 2005 Semiannual Report I Page IO 5.0 Closing Comments The current report presents the results of quarterly CERCLA-related and semiannual PEW-related ground-water sampling at the CNA/Ticona Shelby, NC facility. The next round of samples are scheduled to be collected during the 3rd and 4th Quarters of 2005 and will be included in the next semiannual report to the agencies in March 2006. ------------Kubal-Furr & Associates ------------- I I I I I I Tables I I ' I >~ ,, ' I , ';.~ .. I I ·~/~ ·t ~' •,; ~ I I I I I I I Kubal-Furr & Associates - - -- - - -- -- -- - - Table 1. 2005 Sampling Matrix-CNA Holdings, lnc./Ticona-Shelby, NC 1st Quarter Monitoring Toe voe Location (9060) (82608) Monitor We/Js C-49 .,J K-28 .,J .,J P-58 T-35 .,J V-23 .,J .,J AA-54 CC-33 .,J EE-58 .,J FF-34 FF-62 .,J GG-61 .,J HH-48 HH-77 .,J PEW-Related Same/es PEW-1 .,J PEW-3 .,J PEW-4 .,J F-55 Notes: TOC = Total Organic Carbon VOC ::: Volatile Organic Compounds SVOC = Semivolatile Organic Compounds PEW = Polymer Extraction Well 9060/8260B/8270C = Test methods in SW846 2nd Quarter 3rd Quarter svoe Toe voe svoe Toe voe svoe (8270C) (9060) (82608) (8270C) (9060) (8260B) (8270C) .,J .,J .,J .,J .,J .,J .,J .,J .,J .,J .,J .,J .,J .,J .,J .,J .,J .,J .,J .,J .,J .,J - - - - 4th Quarter Toe voe SVoe (9060) (8260B) (8270C) .,J .,J CNA Holdings, lnc./Ttcona-Shelby, NC OU-I Semiannual Report (Jan. '05 June '05) - - - - - -- - - - - - - - - - Table 2. Summary of Selected CERCLA-Related Water-Quality Constituents (1st Quarter 2005) CNA Holdings, lnc./Ticona-Shelby, North Carolina (All results reported in milligrams per liter [mg/L]) Total Organic Carbon Volatile Organics 2-Butanone (MEK) Acetone Benzene Cis-1 , 2-Dichloroethene Chlorobenzene Ethyl benzene Toluene Trichloroethane Xylenes (total) EPA/NC P-58 ✓ NE/NE NA NE/4.20 <0.0050 NE/0.7 0.0091U · 0.005/0.001 <0.0010 0.0710.07 <0.0010 0.1 /0.05 <0.0010 0.7/0.550 <0.0010 1.0/1.0 <0.0010 0.005/0.0028 <0.0010 10/0.53 <0.0020 Notes: NA = Sample not analyzed for indicated constituents T-35 / V-23 / NA 10700 <0.0050 <0.0050 <0.0050 <0.0050 <0.0010 0.021 · <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 0.0031 • <0.0010 0.010 ' 0.0016 <0.0010 <0.0020 0.012 ' EPA = Environmental Protection Agency National Primary Drinking Water Standards K-28 / 0.084 · 0.12 · 0.0083 · <0.0010 <0.0010 <0.0010 0.0020 · <0.0010 <0.0020 NC = North Carolina Groundwater Quality Standards ( 1 SA NCAC 02L .0202 [April 1, 2005]) NE = Not Established U = Constituent not detected above the associated sample quantitation limit CC-33 / NA <0.0050 <0.0050 <0.0010 0.0022 · 0.0019· <0.0010 <0.0010 <0.0010 <0.0020 - - - HH-48 / HH-77 / NA NA <0.0050 <0.01 5 <0.0050 <0.01 5 <0.0010 <0.0030 <0.0010 <0.0030 <0.0010 <0.0030 <0.0010 <0.0030 <0.0010 <0.0030 0.20 0.38 <0.0020 <0.0060 CNA Holdings, lnc.mcona-Shelby, NC OU-1 Semiannual Report (Jan. '05 -June '05) - - -- -- - - - - - - -- --- - - Notes: Table 3. Summary of Selected CERCLA-Related Water-Quality Constituents (2nd Quarter 2005) CNA Holdings, lnc./Ticona-Shelby, North Carolina (All results reported in milligrams per liter [mg/L]) EPA/NC Total Organic Carbon NE/NE K-28/ 52.7 DUP-2 (K-28)/ 50.1 EPA = Environmental Protection Agency National Primary Drinking Water Standards NC = North Carolina Groundwater Quality Standards (Subchapter 2L) NE= Not Established V-23 ./ 8900 CNA Holdings, lncflicona-Shelby, NC OU-1 Semiannual Report (Jan. '05 -June '05) - - - ----- - - - - - -- - - Table 4. Summary of Selected PEW-Related Water Quality Constituents (1st Quarter 2005) CNA Holdings, lnc./Ticona-Shelby, North Carolina (All results reported in milligrams per liter [mg/L]) EPA/NC F-55 / PEW-1 ✓ DUP-4 (PEW-1)✓ PEW-3 / Semivo/atile Organics 1 , 1 Biphenyl NE/0.35 20.8 · <0.010 <0.010 0.27 · 2-Methylnaphthalene NE/0.0140 0.074 , <0.010 <0.010 <0.010 Biphenyl Ether NE/NE 62.7 · <0.010 <0.010 0.86 · Phenol NE/0.30 0.26J · <0.010 <0.010 <0.010 Volatile Organics Benzene 0.005/0.001 0.051X, <0.0010 <0.0010 <0.0010 Chloroform 0.08/0.07 <0.0030 0.0016 0.0018 • <0.0010 Cis-1,2-Dichloroethene 0.07/0,07 <0.0030 0.0012 0.0012 , <0.0010 Methylene Chloride 0.005/0,0046 0.014X • <0.0010 <0.0010 <0.0010 Toluene Trichloroethene Notes: 1.0/1.0 0.0057X · <0.0010 <0.0010 <0.0010 0.005/0.0028 <0.0030 0.0055 0.0054 • <0.0010 EPA = Environmental Protection Agency National Primary Drinking Water Standards NC= North Carolina Groundwater Quality Standards (15A NCAC OZL .0202 [April 1, 2005)) NE= Not Established DUP = Duplicate Sample J = The analyte was positively identified; the associated numerical value is the approximate concentration of the analyte in the sample. X = Sample diluted due to matrix interference (applied by the laboratory), no affect on data useability - - - - PEW-4 / <0.010 <0.010 0.026 · <0.010 0.0026 · <0.0010 0.0056 <0.0010 <0.0010 0.015 CNA Holdings. /nc.fficona-Shelby, NC OU-I Semiannual Reporr (Jan. '05 -June '05) I I I I I Figures I I I I I I I I I I I I I I Kubal-Furr & Associates -- .. •0 I 0 - - -- - -- - - - 0 350 700 - - - - - - Legend • MonitorWeff 4 Piezomet&r • Surface Water Location • Outer Tier Extraction Well • Inner Tier Extraction Wen ■ PEW Extraction Well a Residential Well ,,,,,--.,," Creek/Stream □ Building I Structure Kubal-Furr & Associates -Environmental Consultants- Figure 1. Site Location Map C.\~ Holdings, lncfficono Shelby, Nonh Carolina - -- - I 0 • 0 Legend MnnttnrWell Water-Level (ft msl) • Inner Tier Extraction Well ,,,,,-...--,, Creek/ Stream (E Building I Structure Inferred Direction of Ground-Water Flow - - -- - ' ' ,. --\ I , ' Recreation Pond - . , I 'S I \ \ \ ' 0 -- t I ' I • ' ' • fb_nn_, __ ~rr.. I . . ! I f .w,~~ -~, 350 -- ~· "· i \ \ \ 0'~~2 ' .... .... '/. ' .... ,,.. .... ' - I \ I I J " ' \ \ I _..-1. • " "' ' - - - - - toner Tier Extraction Well Water-I eve! Elevations I I \ \ I I ' I I • I I I IT-1 = 804.21 IT-2 = 805.25 IT-3 = 802.94 IT-4 = 802.59 IT-5 = 803.74 IT-6 = 804.08 IT-7 = 803.82 IT-SR = 800 .54 IT-9 = 798.05 Kubal-Furr & Associates -Environmental Consultants- Figure 2. Potentiometric Surface Map Shallow Saprolite-February 10, 2005 C\~4 Holdings, lnc.1Ticona Shelb)•, l'l/orth Carolina -- -- ------ - -- ' ,. , -. ' I I 0 ~ ' , ., ..... ~ L \ ' ofs~~ 'J \\ \. .. 'S 0 350 700 - ~ "' ,. ' - - -- \ \ \ I ' \ \ \ ', '• 0 .... Legend "'"""'-"'ell Water-Level (ft msl) Piezometer ❖ Outer Tier Extraction WeB ■ PEW Extraction Well /780/ W~~t.i:!~ur ,,.-..-,, Creek/ Stream □ Buikllng I Structure ..,...,, Inferred Direction of Ground-Water Flow • Water level for well F-55 was measured on 2/18/05 Kubal-Furr & Associates -Environmental Consultants~ Figure 3. Potentiometrlc Surface Map - Deep Saprolite/Upper Bedrock-February 10, 2005 CNA Holdings, /nc.!Ticona Shelby, North Carolina - - - - - - - - - - - --- 850.00 A -~ •~=--=--=--=--=--=--=--=--=--=--~--:~la~nt~A<~•~•:.::=======~r=:::::;:::----------'VVastewater Treatment A.rea------------e 830.00 810.00 79000 770.00 750.00 730.00 710.00 690.00 670.00 D-66 827.16 ,-;,. A,.,._ A A;. A,. A;,. ;. A A,.,.,.,. ,. ,. ,. ,. ,. ,. ,. ,. ,. ,. ,. ,. ,. ,. ,. ,. ,. ,. Legend -8101 Une of equal fluid potential (ft msl) GJ Bedrock (dashed 'Mlel'e rnerred) • -Potentiometric Surface Saprolite G-50 813.61 Inferred direction of ground-water movement Screened Interval of V\lell J-29 808.12 Horizontal Scale in Feet 0 400 800 '- • C ::J i,' ! I GG-25 754.51"" I GG-39 754.25 - - - - A' 650.00 830.00 810.00 790.00 770.00 750.00 730.00 710.00 691100 670.00 Kubal-Furr & Associates -Environmental Consultants - F1gure 4. HJdrogeologlc Cross Section A-A'-February 10, 2005 CNA Holdings. lncfficona Shelby. North Carolina - - - - 0 I 0 0 Legend MoottorWell Water-level (n fMI) • Jnner Tier Extraction Well /?so/ ~~~v:!=ur ..,,,-...-,, Creek I Stream Iii Building/ Strucll,mt _,,, Inferred Direction of Ground-water Flow --- ---- - ', .. - -I . ' I \ \ \ ' ' ~~ m~ \ .... -· .. • 1 II ~1 R,_wn c=i7ii~ ~,™o, " I ! ; f u~:i ... • 0 350 700 - - - I I I I _.I,. I I '- - - - - - Inner Der Extraction Well Water-I eve! Elevations I \ IT-1 = 805.30 IT-2 = 806.24 IT-3 = 803.60 IT-4 = 803.33 IT-5 = 804.24 IT-6 = 804.65 IT-7 = 804.53 IT-SR= 800.12 IT-9 = 798.63 I I I I I I I • □ I ' I I., ..., I, ~ ' . -I '. Kubal-Furr & Associates -Environmental Consultants- Figure 5. Potentiometric Surface Map Shallow Saprolite-May 2, 2005 CNA Holdings. Jnc.!Ticona Shelby, North Carolina - - - - - -- - - - - - \ - ?. •, ' , ' , ,. e ' I , I> I 0 Recreation Pond o~: ---~\ 0 ,00 - - - - --Legend Moaimr Well 0 Water-level (ft msl) ... Piezometer ❖ 0ut8f ner Extraction Well ■ PEW Extraction Well water-Level Contour ,,..,.,,-,, (dloti.a,,,.,.,.1"•~ --Creek f Stream □ Building I Structure ~ Inferred Direction of ""()J.1-1!5 Ground-Water Flow 7~00 .. Water level for well F-55 was \ measured on 5/4/05 \ \ ,)# \ \ I I \ I I I I I I • I I I ~ :,";;'; ,b p;~, ,,.. I I I I ' ,......,.,.. I I I \ Kubal-Furr & Associates -Environmental Consultants- Figure 6. Potentiometric Surface Map Deep Saprollte/Upper Bedrock-May 2, 2005 C."IA Holdings, Inc.lTicona Shelby, North Carolina - - - - - - -- - - - - --- 850.00 A -~•:-=-=-=-=-=-=-=-=-=-=-=-~:l~•:nt'..Ar~•~•========~r=:::::::::------------11/V-astewaterTreatmentArea-----------<1 630.00 810.00 790.00 770.00 750.00 730.00 710.00 690.00 670.00 • 0-27 828.43 D-35 828.06 D-56 828.06 Legend _5101 Line of equal fluid potential (ft msl) GJ Bedrock (dashed ~e lllf"erred} Potentiometric Surface Saprolite G--50 813.93 Inferred direction of ground-water movement Screened Interval ofVVell ~ ,----, J-29 809.16 Horizontal Scale in Feet 0 400 '-.. " 800 ' " • C ::, i, • ~ e a. I I ' GG-25 755.53~ I GG-39 755.23 - -- - A' 850.00 830.00 810.00 790.00 770.00 750.00 730.00 710.00 690.00 670.00 Kubal-Furr & Associates -Environmental Consultants - Flgure 7. Hydrogeologlc Cros..<1 Section A-A'-:\lay 2, ZOOS CNA Holdings, /nc.fTicoria Shelby, North Carolina - I I I I I I I I I I I I I I I I I I I Attachment 1 Analytical Data Package, Data Assessment Summary and Field Sampling Logs for the 1st and 2nd Quarter 2005 Sampling Events -----------Kubal-Furr & Associates ----------- I I I I I I I I I I I I I I I I I I I DATA ASSESSMENT SUMMARY CHECKLIST AND REPORT-LEVEL II Client ID: Project Number: Project Description: Ticona, Shelby, NC 26RP21 01/05 Sample Delivery Group (SDG) Description: Prepared By: Robert DeGaetano Date: 07 /12/05 Seventeen aqueous samples, one field duplicate, four trip blanks and a field blank were collected by Kubal-Furr & Associates and submitted to Davis & Floyd of Greenwood, SC for analysis. The samples were tested for volatiles, semivolatiles, Dow Therm A parameters ( I, 1-biphenyl and biphenyl ether) and total organic carbon. The laboratory login numbers were L0502 I 805, L05022007, L05022303, L05022401 and L05022812. - CONTENTS LEVEL COMMENTS II Sample Results ✓ Most data considered Class A as reported. Some data are considered Class B, and are assigned qualifiers. Chain(s) of Custody (COCs) ✓ See Discussion Master Tracking List ✓ Satisfactory Method Conformance Summary ✓ Satisfactory Batch Quality Control Report ✓ Satisfactory Trip/Field/Equipment Blank Report ✓ Acetone detected in the field blank Field Notes/Logbook ✓ Not reviewed Discussion: Acetone was detected in the field blank collected on 2/22/05 at a concentration of 0.0 I 6 mg/L. Consequently, the acetone result for sample P-58 was flagged with a "U" qualifier. The acetone result for K-28 (0.12 mg/L) was not qualified, however, due to the presence of this parameter detected at the same concentration (0.12 mg/L) in March 2004. The phenol result for field sample F-55 was flagged with a "J" qualifier due to low (<! 0%) recovery of the surrogate and recovery values for phenol in the associated MS/MSD samples that exceeded control limits. The reporting limits for the volatiles analysis of field samples HH-77 and F-55 were raised due to matrix interference. Class A = quantitative Class B = qualitative Class C = unuseable Kubal-Furr & Associates I I I I I I I I I I I I I I I I I I I DAYIS FL6YD April 18, 2005 PEM CARTER TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report ID : AC1040 Page 1 of 88 LABORATORY ANALYSIS REPORT Login Number Project Number Description :L05021803, L05021805, L05022007, L05022303, L05022401, L05022812 :61621.01 :GROUNDWATER-PROJECT #TF026QS15 Dear Pem Carter: We are pleased to provide the enclosed analytical results for the samples received by Davis & Floyd, Inc. on February 17, 2005 through February 24, 2005. A formal Quality Assurance/Quality Control program is maintained by Davis & Floyd, which is designed to meet or exceed the EPA, NELAC or other appropriate regulatory requirements. All analytical analyses for this project met QA/QC criteria and the results are within the 99 % confidence interval for each method unless otherwise stated in the footnotes. This report is to be reproduced only in full. Feel free to contact our Client Services Representative at (864) 229-4413 if further explanation of the analysis is required. Unless other arrangements have been made, samples will be disposed of or returned 14 days from the cfate of the report. We appreciate the opportunity to provide services to your firm. Sincerely, DAVI~/4INC ohn H. McCord, Jr. Laboratory Manager !J;wis 8, f-loyd, Inc. I PO Drawer 42B I Greenwood, SC 29(i4c3 I 13 I h E. Durst Avenue i Creenwoorl, SC 206-1~1 I (3(,4) 22Y-4413 I Fax (8(,4) 229-71 19 DAYIS FLtfYD Client Contact LABORATORY ANALYSIS REPORT TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Certification Number: 25 Project Number: 61621.01 Report Date Page 2 of 88 April 18, 2005 Report ID: AC1040 Master Sample Tracking List Sample ID L0S0:.nso3-01 Volatile Organics SW846 8260B L05021803-06 Volati,10 Organics SW846 8260B L05021805-0l Volatile Organics SW846 8260B L05021805-02 Volatile Organics SW846 8260B L05021805-03 Volatile Organics SW846 8260B L05021805-04 Volatile Organics SW846 8260B L05021805-05 Volatile Organics SW846 8260B L05021805-06 Volatile Organics SW846 8260B Client ID Date Collected Date Received DUP-1 02/24/2005 0837 EB-01 02/16/2005 1351 02/24/2005 0819 HH-77 02/22/2005 1556 HH-48 02/15/2005 1354 02/17/2005 02/22/2005 1328 02/22/2005 1346 FP'-34 02/22/2005 1405 P'P-62 1705 02/22/2005 1424 GG-61 1032 02/22/2005 1442 Dcwls & Floyd, Inc. I PO Dr:1wer 428 I Creenwond, SC 2%48 I 816 E. Durst t\venue I Greenwood, SC 29649 I (864) 229-4413 I Fax (864) 229-7 l 19 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAYIS FLrnlD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter Master Sample Tracking List Sample ID L05021805-07 Volatile Organics SW846 8260B L0S0J:1805-08 n1n:n::~;1ni;;,r;;¥1Mw Yolati_l'II' Organics SW846 8260B L05021805-09 Volatile Organics SW846 8260B L05021805-10 Volatile Organics SW846 8260B L05022007-0l Volatile Organics SW846 8260B L05022007-02 l!tffil~iit#til!iiiil£i1Il Semivolatile Organics SW846 8270C SW846 8270C SW846 8270C DOWTHERM SW846 8270C DOWTHERM Volatile organics SW846 8260B L05022007-03 Volatile Organics SW846 8260B Client ID AA-54 BB-58 TRIP BLANK P-58 l"-55 CC-33 SW846 3510C SW846 3510C SW846 3500B SW846 3500B NC Cenijication Number: 25 Project Number: 61621.01 Report Date Page 3 of 88 Date Collected Ol/1'/2005 1033 02/03/2005 1450 Ol/18/1005 1355 02/22/2005 0800 02/22/2005 0800 02/22/2005 0800 02/22/2005 0800 April 18, 2005 Report ID: AC1040 Date Received 02/22/2005 1501 02/17/2005 02/22/2005 1519 02/17/2005 02/22/2005 1538 02/17/2005 02/24/2005 0743 02/21/2005 1544 02/11/20011 IM!U~UitRi.#.~(#\Ht: 03/01/2005 1845 03/02/2005 1256 03/01/2005 1806 03/01/2005 1845 02/21/2005 1620 02/21/2005 1602 0;1vis & Floyd, Inc. I PO Drciwcr 428 I Crcenwood, SC 291,,18 I ll 16 E. Dt1rst Avenue I Cree11wood, SC 29(i49 I (8fl4) 22:J-441 J I fax (8(,4) 22'J-7 \ ·1 ~ Dl\:YIS FL(}YD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem carter Master Sample Tracking List Sample ID L05022007-04 Volatile Organics SW846 8260B L05022303-0l m::i:mn~;ifli;;1n;;@JMtm s .. iYoi~til• Organics SW846 827DC SW846 8270C DOWTHERM Volatile Organics SW846 8260B Semivolatile Organics SW846 8270C SW846 B270C DOWTHERM SW84 6 8270C DOWTHERM Volatile organics SW846 8260B L05022303-03 Semivolatile Organics SW846 8270C SW846 8270C DOWTHERM Volatile Organics SW846 8260B LOS022303-04 Semivolatile Organics SW846 8270C SW846 8270C DOWTHERM Volatile Organics SW846 8260B Client ID TRIP BLANK-2 PBW-1 1Hf!fFff;;::::;;Jg;;:; PEW-4 DUP-4 SW846 3510C SW846 35008 SW846 3510C SW846 3500B SW846 3500B SW846 3510C SW846 35008 SW846 3510C SW846 3500B NC Certification Number: 25 Project Number: 61621.01 Report Date Page 4 of 88 Date Collected 02/22/2005 1343 April 18, 2005 Report ID: AC1040 Date Received 02/21/2005 1204 02/.ll/:z00.5 !?fKlFlFfif!tit;t::Mt?; tttitthtJJtf?tffM!Xi:rtt¥Jii!Jft>r?rr::::,::·:-: 02/28/2005 0800 02/28/2005 0800 1453 02/28/2005 0800 02/28/2005 0800 02/28/2005 0800 1443 02/28/2005 0800 02/28/2005 0800 02/28/2005 0800 02/28/2005 0800 03/03/2005 1238 03/03/2005 1238 02/24/2005 0856 03/03/2005 1515 03/03/2005 1438 03/03/2005 1756 02/24/2005 0915 02/l2/2005 03/03/2005 1557 03/03/2005 1557 02/24/2005 0933 03/03/2005 1636 03/03/2005 1636 02/24/2005 0951 Dcwis & Floyd, Inc I PO Drawer 428 I Creenwood, SC 21J64B I HI G F.. Durst Avcnu~ I Cmenwood, SC 2%49 I (864) 22~-441 '.\ I F;ix (864) 229-71 t 9 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I 0~11s FLOYD LABORATORY ANALYSIS REPORT Client Contact TICONA, LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 2B152 Pem Carter NC Certification Number: 25 Project Number: 61621.01 Report Date Page s of BB April 18, 2005 Report ID: AC1040 Master Sample Tracking List Sample ID L05022303-05 Volatile Organics SW846 8260B L05022401-01 Client ID TRIP BLANK-3 V-23 @t:nm:;w.i;H;~m:~u~~~at :::::::::::;:;tt:t:Jttt::=+~¥.;1:r•'.®.;~ Volatile Organics SW846 8260B Wet Chemistry SW846 9060 L05022401-02 Volatile Organics SW846 8260B Wet Chemistry SW846 9060 JC-28 L05022401-03 TRIP BLANK-4 :n:n:ntMARW£~@1i1M¥trn:n:n:n:n:n:n:n::n:i:,1;1r;;:~~m: Volatile Organics SW846 8260B L05022812-01 Semivolatile Organics SW846 8270C SW846 8270C DOWTHERM Volatile Organics SW846 8260B PB-01 SW846 3510C SWB46 3500B Date Collected 0900 02/23/2005 0945 ?dttftffft/:H?t!t;;i(~~.~,id 02/22/2005 1715 02/01/200.5 0900 iiif~ji~~i~\l:li 02/22/2005 1745 02/28/2005 0800 02/28/2005 0800 Date Received 02/24/2005 0801 02/ll/2005 :n:4-~_!Y.it~t~~itt 02/24/2005 1246 03/03/2005 2002 02/24/2005 1343 03/03/2005 2027 02/23/2005 nrrrnu~ii;~nr¥.;.t:;:r 02/24/2005 02/24/2005 1227 03/03/2005 1715 03/03/2005 1715 03/03/2005 1216 Davis & Flnyd, Inc. I PO Drawer 428 I Greenwood, SC 2964H I 81 h E. Durst Avenue I Greenwood, SC 29649 I {864) 22.9-4413 I Fax (864) 219-7119 I LABORATORY ANALYSIS REPORT I I NC Certification Number: 25 Client TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 I Contact Pem Carter Page 6 of 88 Report ID: AC1040 Client ID: DUP-1 Sample ID L05021803-01 Date Collected: 02/16/2005 0000 I Matrix GW/ChemW Date Received 02/17/2005 Parameter Result Qual RDL Units Analyst Date Time I Volatile organics SW846 8260B 1,1,1-TRICHLOROETHANE ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 0837 I 1,1,2,2-TETRACHLOROETHANE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0837 1,1,2-TRICHLOROETHANE ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 0837 1, 1-DICH_LOROETHANE ' o. 0010 0 .0010 mg/1 PAP 02/24/2005 0837 1 , 1-DI.CHLOROETHENE ' 0.0010 0. 0010 mg/1 PAP 02/24/2005 0837 I 1,2-DICHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0837 1,2-DICHLOROPROPANE ' 0 . 0010 0.0010 mg/1 PAP 02/24/2005 0837 2-BUTANONE ' 0. 0050 0.0050 mg/1 PAP 02/24/2005 0837 2-HEXANONE ' 0. 0050 0.0050 mg/1 PAP 02/24/2005 0837 I 4-METHYL-2-PENTANONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0837 ACETONE ' 0 .0050 0.0050 mg/1 PAP 02/24/2005 0837 BENZENE ' o. 0010 0.0010 mg/1 PAP 02/24/2005 0837 I BROMODICHLOROMETHANE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0837 BROMOFORM ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0837 BROMOMETHANE ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 0837 CARBON DISULFIDE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0837 I CARBON TETRACHLORIDE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0837 CHLOROBENZENE ' o. 0010 0.0010 mg/1 PAP 02/24/2005 0837 CHLOROETHANE ' 0 . 0010 0.0010 mg/1 PAP 02/24/2005 0837 CHLOROFORM ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 0837 I CHLOROMETHANE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0837 CIS-1,2-DICHLOROETHENE ' 0 . 0010 0.0010 mg/1 PAP 02/24/2005 0837 CIS-1,3-DICHLOROPROPENE ' o. 0010 0.0010 mg/1 PAP 02/24/2005 0837 I DIBROMOCHLOROMETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0837 ETHYLBENZENE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0837 METHYLENE CHLORIDE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0837 STYRENE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0837 I TETRACHLOROETHENE ' 0 .. 0010 0.0010 mg/1 PAP 02/24/2005 0837 TOLUENE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0837 TRANS-1,2-DICHLOROETHENE ' 0 . 0010 0.0010 mg/1 PAP 02/24/2005 0837 TRANS-1,3-DICHLOROPROPENE ' o. 0010 0 .0010 mg/1 PAP 02/24/2005 0837 I TRICHLOROETHENE ' 0 .0010 0. 0010 mg/1 PAP 02/24/2005 0837 VINYL ACETATE ' 0.0010 0 . 0010 mg/1 PAP 02/24/2005 0837 VINYL CHLORIDE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0837 I XYLENE (TOTAL) ' 0.0020 0.0020 mg/1 PAP 02/24/2005 0837 I Davis 81 Floyd, Inc. I PO D1awer 42H ) Greenwood, SC 2%48 I 816 I::. Durst Avenue I Greenwnod, 5C 29G4'.J I (HM) 229-4413 I f-.ix (8fi4) 22<:l-7119 I I I I I I I I I I I I I I I I I I I I Dl\VIS FLffl[D Client Contact Client Matrix Parameter Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE ID: 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICHLQROETHANE 1,1-DICHLOROETHANE 1,1-DLCHLOROETHENE 1,2-DICHLOROETHANE l·, 2-DICHLOROPROPANE 2-BUTANONE 2-HEXANONE 4-METHYL-2-PENTANONE ACETONE BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) LABORATORY ANALYSIS REPORT NC Cenijication Number: 25 TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Pem Carter Page 7 of 88 Report ID: AC1040 BB-01 Sample ID L05021803-06 Date Collected: 02/16/2005 1351 GW/Chemw Date Received 02/17/2005 Result Qual RDL Units Analyst Date Time < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0 0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0 0050 0.0050 mg/1 PAP 02/24/2005 0819 < 0.0050 0.0050 mg/1 PAP 02/24/2005 0819 < 0.0050 0.0050 mg/1 PAP 02/24/2005 0819 o. 011 0.0050 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0 0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0. 0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0 0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0 .0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0 .0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0 .0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0. 0010 0.0010 mg/1 PAP 02/24/2005 0819 < 0.0020 0.0020 mg/1 PAP 02/24/2005 0819 D3vis & Floyd, lnc. I PO Drawer 4213 I Cret:nwood, SC 2964H I 81 fi E. Durst Avenue I Greemvnod, SC 29()49 I (8G4) 229-44.U I Fax (864) 229-71 19 DAYIS FLtrYD Client Contact Client ID: Matrix Parameter Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICHLOROETHANE 1,1-DIC~LOROETHANE 1,1-DICHLOROETHENE 1,2-DICHLOROETHANE 1', 2-DICHLOROPROPANE 2-BUTANONE 2-HEXANONE 4-METHYL-2-PENTANONE ACETONE BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE. CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) LABORATORY ANALYSIS REPORT NC Cenificarion Number: 25 TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report. Date April 18, 2005 Pem Carter Page a of 88 Report ID: AC1040 HH-77 Sample ID L05021805-01 Date Collected: 02/15/2005 1255 GW/Chemw Date Received 02/17/2005 Result Qual RDL Units Analyst Date Time < 0.0030 X 0 . 0030 mg/1 PAP 02/22/2005 1556 < 0.0030 X 0 .0030 mg/1 PAP 02/22/2005 1556 < 0.0030 X 0 . 0030 mg/1 PAP 02/22/2005 1556 < 0.0030 X 0 .0030 mg/1 PAP 02/22/2005 1556 < 0.0030 X o. 0030 mg/1 PAP 02/22/2005 1556 < 0.0030 X 0.0030 mg/1 PAP 02/22/2005 1556 < 0.0030 X 0.0030 mg/1 PAP 02/22/2005 1556 < 0 .015 X 0 .015 mg/! PAP 02/22/2005 1556 < 0 .015 X 0 .015 mg/1 PAP 02/22/2005 1556 < 0 .015 X 0.015 mg/1 PAP 02/22/2005 1556 < 0.015 X 0.015 mg/1 PAP 02/22/2005 1556 < 0 .0030 X 0.0030 mg/1 PAP 02/22/2005 1556 < 0 .0030 X 0.0030 mg/1 PAP 02/22/2005 1556 < 0 .0030 X 0. 0030 mg/1 PAP 02/22/2005 1556 < 0. 0030 X 0 . 0030 mg/! PAP 02/22/2005 1556 < 0. 0030 X o. 0030 mg/1 PAP 02/22/2005 1556 < 0. 0030 X 0.0030 mg/! PAP 02/22/2005 1556 < 0.0030 X 0. 003 0 mg/1 PAP 02/22/2005 1556 < 0.0030 X 0. 003 0 mg/1 PAP 02/22/2005 1556 < 0.0030 X 0.0030 mg/! PAP 02/22/2005 1556 < 0 .0030 X 0.0030 mg/1 PAP 02/22/2005 1556 < 0 . 0030 X 0 . 0030 mg/1 PAP 02/22/2005 1556 < 0 . 0030 X 0 . 0030 mg/1 PAP 02/22/2005 1556 < o. 0030 X 0.0030 mg/1 PAP 02/22/2005 1556 < 0 .0030 X 0.0030 mg/1 PAP 02/22/2005 1556 < 0 .0030 X 0.0030 mg/1 PAP 02/22/2005 1556 < 0.0030 X 0. 003 0 mg/! PAP 02/22/2005 1556 < 0.0030 X 0.0030 mg/1 PAP 02/22/2005 1556 < 0.0030 X 0.0030 mg/1 PAP 02/22/2005 1556 < 0 .0030 X 0.0030 mg/1 PAP 02/22/2005 1556 < 0 .0030 X 0.0030 mg/1 PAP 02/22/2005 1556 0.38 0.0030 mg/1 PAP 02/22/2005 1556 < 0.0030 X 0.0030 mg/1 PAP 02/22/2005 1556 < 0 .0030 X 0. 003 0 mg/1 PAP 02/22/2005 1556 < 0 .0060 X 0.0060 mg/1 PAP 02/22/2005 1556 1);1vi~ & Floyd, Inc. I PO Drawer 428 I Creenwood, SC 29fi41l I !YI 6 I:. Durst Avenue I Crcenwo1Jd, SC 2%4~) I (/l64) 22Y-441] I Fax (81i4) 229-71 1 Y I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAYIS FLMD Client Contact Client ID: Matrix ' Parameter Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICHLOROETHANE 1, 1-DICH,LOROETHANE '' 1,1-DLCHLOROETHENE 1,2-DICHLOROETHANE 1·, 2-DICHLOROPROPANE 2-BUTANONE 2-HEXANONE 4-METHYL-2-PENTANONE ACETONE BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETIWIE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRA.NS-1,3-DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) LABORATORY ANALYSIS REPORT NC Certification Number: 25 TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Pem Carter Page 9 of 88 Report ID: AC1040 HH-48 Sample ID L05021805-02 Date Collected: 02/15/2005 1354 GW/ChemW Date Received 02/17/2005 Result Qual RDL units Analyst Date Time < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0050 0.0050 mg/1 PAP 02/22/2005 1328 < 0.0050 0.0050 mg/1 PAP 02/22/2005 1328 < 0.0050 0.0050 mg/1 PAP 02/22/2005 1328 < 0.0050 0.0050 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/.2005 1328 < 0.0010 0.0010 mg/1 PAP 0.2/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < o. 0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 o. 0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 0.20 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1328 < 0.0010 0 . 0010 mg/1 PAP 02/22/2005 1328 < 0.0020 0. 002 0 mg/1 PAP 02/22/2005 1328 D;1vis & Fluyd, Inc. I !'0 Druwcr 42H I C1ccnwood, SC 2%4/-1 I a 16 E. lJur~t Avenue I Cn~enwood, SC 'J.9649 I (1Hi4} 229-4413 I r'ax (8fi4) 229-711 Y DAYIS FLbYD Client Contact Client ID: Matrix Parameter Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICHLOROETHANE 1, 1-DICH_LOROETHANE 1, 1-DI.CHLOROETHENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 2-BUTANONE 2-HEXANONE 4-METHYL-2-PENTANONE ACETONE BENZENE BROMODICHLOROMETI-WfE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) LABORATORY ANALYSIS REPORT NC Certification Number: 25 TICONA,LLC Project Number; 61621. 01 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 1B, 2005 Pem Carter Page 10 of 88 Report ID: AC1040 C-49 Sample ID L05021805-03 Date Collected: 02/15/2005 1500 GW/ChemW Date Received 02/17/2005 Result Qual RDL units Analyst Date Time ' 0. 0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0 . 0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 134 6 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 134 6 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0. 0050 0.0050 mg/1 PAP 02/22/2005 134 6 ' 0.0050 0.0050 mg/1 PAP 02/22/2005 1346 ' 0 .0050 0.0050 mg/1 PAP 02/22/2005 1346 ' 0 . 0050 0.0050 mg/1 PAP 02/22/2005 1346 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0.0010 0 .0010 mg/1 PAP 02/22/2005 1346 ' 0.0010 0 . 0010 mg/1 PAP 02/22/2005 134 6 ' 0.0010 o. 0010 mg/1 PAP 02/22/2005 1346 ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0. 0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0 .0010 0. 0010 mg/1 PAP 02/22/2005 1346 ' o. 0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0 .. 0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 134 6 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0.0010 0. 0010 mg/1 PAP 02/22/2005 1346 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1346 ' 0.0020 0. 002 0 mg/1 PAP 02/22/2005 1346 Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I HHi E. Durst Avenue I Creenwood, SC 2%49 I (f.164) 229-44 U I F,1x (864) 229-7119 I I I I I I 11 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAjlS FLOYD Client Contact Client Matrix Parameter Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE ID: 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICHLOROETHANE 1,1-DICHLOROETHANE 1, 1-orCH.LOROETHENE 1,2-DICHLOROETHANE 1·, 2-DICHLOROPROPANE 2-BUTANONE 2-HEXANONE 4-METHYL-2-PENTANONE ACETONE BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) LABORATORY ANALYSIS REPORT NC Certification Number: 25 TICONA,LLC Project Number: 61621. 01 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Pem Carter Page 11 of 88 Report ID: AC1040 FF-34 Sample ID L05021805-04 Date Collected: 02/15/2005 1619 GW/ChemW Date Received 02/17/2005 Result Qual RDL Units Analyst Date Time < 0 .0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0 .0010 0. 0010 mg/1 PAP 02/22/2005 1405 < 0 .0010 0. 0010 mg/1 PAP 02/22/2005 1405 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0.0050 0.0050 mg/1 PAP 02/22/2005 1405 < 0.0050 0.0050 mg/1 PAP 02/22/2005 1405 < 0.0050 0.0050 mg/1 PAP 02/22/2005 1405 < 0.0050 0.0050 mg/1 PAP 02/22/2005 1405 < 0.0010 0.0010 mg/1 PAP 02/2:2/2005 1405 < 0. 0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0 0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0 0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0 .0010 0.0010 mg/1 PAP 02/22/2005 1405 < o. 0010 0.0010 mg/1 PAP 02/22/2005 1405 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0 0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0 0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0 .0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0 . 0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0. 0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1405 < 0.0020 0.0020 mg/1 PAP 02/22/2005 1405 D.ivis & r:loyd, Inc. I PO Drawer 428 j Greenwood, SC ~9648 I 816 1-:. Dur.<-t Avenu,~ I Greenwood, SC ~9649 I (864) 229-4413 I Fax (864) 229-71 I~ I LABORATORY ANALYSIS REPORT I I NC Certification Number: 25 Client TICONA,LLC Project Number: 61621.01 I 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 I Contact Pem Carter Page 12 of 88 Report ID: AC1040 Client ID: l"F-62 Sample ID L05021805-05 Date Collected: 02/15/:2005 1705 I Matrix ' GW/ChemW Date Received 02/17/2005 Parameter Result Qual RDL Units Analyst Date Time I Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE ' o. 0010 0 . 0010 mg/1 PAP 02/22/2005 1424 I 1,1,2,2-TETRACHLOROETHANE ' 0 .0010 0 .0010 mg/1 PAP 02/22/2005 1424 1,1,2-TRICHLOROETHANE ' 0 .0010 0. 0010 mg/1 PAP 02/22/2005 1424 1,1-DICHLOROETJ-W.l"E ' 0 . 0010 0. 0010 mg/1 PAP 02/22/2005 1424 l,1-DICHL0ROETHENE ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1424 I 1,2-DICHLOROETHANE ' 0.0010 0 .0010 mg/1 PAP 02/22/2005 1424 1,2-DICHLOROPROPANE ' 0.0010 0. 0010 mg/1 PAP 02/22/2005 1424 2-BUTANONE ' 0 . 0050 0.0050 mg/! PAP 02/22/2005 1424 2-HEXANONE ' 0 .0050 0 .0050 mg/1 PAP 02/22/2005 1424 I 4-METHYL-2-PENTANONE ' 0 .0050 o. 0050 mg/1 PAP 02/22/2005 1424 ACETONE ' 0.0050 0.0050 mg/1 PAP 02/22/2005 1424 BENZENE . ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1424 I BROMODICHLOROMETHANE ' 0. 0010 0.0010 mg/1 PAP 02/22/2005 1424 BROMOFORM ' o. 0010 0.0010 mg/1 PAP 02/22/2005 1424 BROMOMETHANE ' 0 .0010 0 . 0010 mg/1 PAP 02/22/2005 1424 CARBON DISULFIDE ' 0 .0010 0 .0010 mg/1 PAP 02/22/2005 1424 I CARBON TETRACHLORIDE ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1424 CHLOROBENZENE ' o. 0010 0.0010 mg/1 PAP 02/22/2005 1424 CHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1424 CHLOROFORM ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1424 I CHLOROMETHANE ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1424 CIS-1,2-DICHLOROETHENE ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1424 CIS-1,3-0ICHLOROPROPENE ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1424 I DIBROMOCHLOROMETHANE ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1424 ETHYLBENZENE ' 0 .0010 0.0010 mg/! PAP 02/22/2005 1424 METHYLENE CHLORIDE ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1424 STYRENE ' 0. 0010 0.0010 mg/1 PAP 02/22/2005 1424 I TETRACHLOROETHENE ' 0 .0010 0 . 0010 mg/1 PAP 02/22/2005 1424 TOLUENE ' o. 0010 0 . 0010 mg/1 PAP 02/22/2005 1424 TRANS-1,2-DICHLOROETHENE ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1424 TRANS-1,3-DICHLOROPROPENE ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1424 TRICHLOROETHENE ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1424 VINYL ACETATE ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1424 VINYL CHLORIDE ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1424 XYLENE (TOTAL) ' 0.0020 0.0020 mg/1 PAP 02/22/2005 1424 I Davis 8, Floyd, Inc. I PO Orc1wer 428 I Greenwood, SC 2%413 I WI 6 t. Durst Avenue I Creenwuod, SC 29649 I (864) 22'.)-441 :l I Fax (8h4) 22'.l-7I1 '.J I I I I I I I I I I I I I I I I I I I I DAYIS FLOYD Client Contact Client Matrix Parameter Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE ID: 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICHLOROETHANE 1,1-DICHLOROETHANE 1,1-DI~HLOROETHENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 2-BUTANONE 2-HEXANONE 4-METHYL-2-PENTANONE ACETONE BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS·l,2·DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3·DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) LABORATORY ANALYSIS REPORT NC Cenification Number: 25 TICONA,LLC Project Number: 61621. 01 2525 BLACKSBURG ROAD HWY 198 SHELBY. NC 28152 Report Date April 18, 2005 Pem Carter Page 13 of 88 Report ID: AC1040 GG-61 Sample ID L05021805-06 Date Collected: 02/16/2005 1032 GW/ChemW Date Received 02/17/2005 Result Qual RDL Units Analyst Date Time < 0.0010 0 .0010 mg/1 PAP 02/22/2005 1442 < 0.0010 o. 0010 mg/1 PAP 02/22/2005 1442 < 0.0010 o. 0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0 0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0 0010 mg/1 PAP 02/22/2005 1442 < 0.0050 0 0050 mg/1 PAP 02/22/2005 1442 < 0.0050 0 0050 mg/1 PAP 02/22/2005 1442 < 0.0050 0 0050 mg/1 PAP 02/22/2005 1442 < 0.0050 0 .0050 mg/1 PAP 02/22/2005 1442 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0 0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0 0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0 0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0 0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0 . 0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1442 < o. 0010 0. 0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0 .0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0 . 0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0. 0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0 .0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0. 0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1442 < 0. 0020 0.0020 mg/1 PAP 02/22/2005 1442 Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I Hl 6 E. Durst Avenue I Greenwonrl. SC 29649 I (8641 229-4413 I Fax (864) 229-71 19 DAYIS FLtfYD Client Contact Client Matrix Parameter Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE ID: 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICHLOROETHANE 1,1-DICHLOROETHANE 1, 1-DI,c°HLOROETHENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 2-BUTANONE 2-HEXANONE 4-METHYL-2-PENTANONE ACETONE BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLO RO ETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) LABORATORY ANALYSIS REPORT NC Certification Number: 25 TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Pem Carter Page 14 of 88 Report ID: AC1040 T-35 Sample ID L05021805-07 Date Collected: 02/16/2005 1240 GW/ChemW Date Received 02/17/2005 Result Qual RDL Units Analyst Date Time < 0.0010 0.0010 mg/1 PAP 02/22/2005 1501 < 0.0010 0 .0010 mg/1 PAP 02/22/2005 1501 < 0.0010 o. 0010 mg/1 PAP 02/22/2005 1501 < 0.0010 0. 0010 mg/1 PAP 02/22/2005 1501 < 0 .0010 0.0010 mg/1 PAP 02/22/2005 1501 < 0 .0010 0.0010 mg/1 PAP 02/22/2005 1501 < 0 .0010 0.0010 mg/1 PAP 02/22/2005 1501 < 0 .0050 0.0050 mg/1 PAP 02/22/2005 1501 < 0 .0050 0.0050 mg/1 PAP 02/22/2005 1501 < 0.0050 0.0050 mg/1 PAP 02/22/2005 1501 < 0.0050 0.0050 mg/1 PAP 02/22/2005 1501 < 0.0010 0. 0010 mg/1 PAP 02/22/2005 1501 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1501 < 0.0010 0 .0010 mg/1 PAP 02/22/2005 1501 < 0.0010 0 .0010 mg/1 PAP 02/22/2005 1501 < 0.0010 0 . 0010 mg/1 PAP 02/22/2005 1501 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1501 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1501 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1501 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1501 < 0.0010 0 .0010 mg/1 PAP 02/22/2005 1501 < 0.0010 0 . 0010 mg/1 PAP 02/22/2005 1501 < 0 . 0010 o. 0010 mg/1 PAP 02/22/2005 1501 < 0 .0010 0.0010 mg/1 PAP 02/22/2005 1501 < 0. 0010 0.0010 mg/1 PAP 02/22/2005 1501 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1501 0.0010 0. 0010 ' < mg/1 PAP 02/22/2005 1501 < 0:0010 0.0010 mg/1 PAP 02/22/2005 1501 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1501 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1501 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1501 0.0016 0. 0010 mg/1 PAP 02/22/2005 1501 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1501 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1501 < 0.0020 0.0020 mg/1 PAP 02/22/2005 1501 Davis & Floyd, Inc. I PO Drawer 42H / Greenwood. SC 29648 I B 16 E. Durst Avenue I Greenwood, SC 2%49 ) (flfJ4) 229-4413 I fax (1ff,4J 229-7119 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I D:\YIS FLOYD Client Contact Client Matrix Parameter Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE ID: 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICHLOROETHANE 1,1-DICH~ROETHANE 1,1-DICHLOROETHENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 2-BUTANONE 2-HEXANONE 4-METHYL-2 PENTANONE ACETONE BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHE~E CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) LABORATORY ANALYSIS REPORT NC Cenijication Number: 25 TICONA,LLC Project Number: 61621. 01 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Pem Carter Page 15 of 88 Report ID: AC1040 AA-54 Sample ID L05021BOS~OB Date Collected: 02/16/2005 1033 GW/Chemw Date Received 02/17/2005 Result Qual RDL Units Analyst Date Time ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0050 0.0050 mg/1 PAP 02/22/2005 1519 ' 0.0050 0.0050 mg/1 PAP 02/22/2005 1519 ' 0.0050 0.0050 mg/1 PAP 02/22/2005 1519 ' 0.0050 0.0050 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0 0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' o._0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0 . 0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519 ' 0.0020 0. 002 0 mg/1 PAP 02/22/2005 1519 Davis & Floyd, Inc. I PO Dr<1wer 428 I Creenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, 5C 29649 I (ll(,4) 229-4413 I Fax (864) 229-7119 DAYIS FLfrYD Client Contact Client Matrix Parameter Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE ID: 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICHLOROETHANE 1,1-DICHLOROETHANE 1, 1-Dr,cHLOROETHENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 2-BlITANONE 2-HEXANONE 4-METHYL-2-PENTANONE ACETONE BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) LABORATORY ANALYSIS REPORT NC Certification Number: 25 TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Pem Carter Page 16 of 88 Report ID: AC1040 EB-58 Sample ID L05021805-09 Date Collected: 02/16/2005 1153 GW/ChemW Date Received 02/17/2005 Result Qual RDL Units Analyst Date Time < 0.0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0.0010 0.0010 mg/1 PAP 02/22/2005 153 8 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0. 0010 0. 0010 mg/1 PAP 02/22/2005 1538 < 0.0050 0.0050 mg/1 PAP 02/22/2005 1538 < 0.0050 0.0050 mg/1 PAP 02/22/2005 1538 < 0.0050 0.0050 mg/1 PAP 02/22/2005 1538 < 0 .0050 0.0050 mg/1 PAP 02/22/2005 153 8 < 0. 0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0 0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0 .0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0. 0010 0.0010 mg/1 PAP 02/22/2005 1538 < o. 0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0 0010 o. 0010 mg/1 PAP 02/22/2005 1538 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0.0010 0 0010 mg/1 PAP 02/22/2005 1538 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0 .0010 0.0010 mg/_1 PAP 02/22/2005 1538 < 0. 0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0. 0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0 0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0 ._0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0. 0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0. 0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0 0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0 0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0 .0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0.0010 0.0010 mg/1 PAP 02/22/2005 1538 < 0.0020 0. 002 0 mg/1 PAP 02/22/2005 1538 Davis & Floyd, Inc. I PO Druwer 428 I Greenwood. SC 2%413 I 81 (i E. Durst Avenue I Greenwood. SC 29649 I (804) 229-441 '.I I Fax (804) 229-7119 I I I I I I I I I I I I 11 I 1! I I I I I I I I I I I I I I I I I I I I I I I D~IS FLOYD Client Contact Client Matrix Parameter Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE ID: 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICHLOROETHANE 1, 1-DICH,LOROETHANE 1, 1-DI,CHLOROETHENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 2-BUTANONE 2-HEXANONE 4-METHYL-2-PENTANONE ACETONE BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) LABORATORY ANALYSIS REPORT NC Cenification Number: 25 TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Pem Carter Page 17 of BB Report ID: AC1040 TRIP BLANlC Sample ID LOS021805-10 Date Collected: 02/03/2005 1450 GW/Chemw Date Received 02/17/2005 Result Qual RDL Units Analyst Date Time ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0 .0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0743 ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0743 ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0743 ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0. 0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0: 0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0. 0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0 . 0010 0.0010 mg/1 PAP 02/24/2005 0743 ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0743 ' o. 0020 0.0020 mg/1 PAP 02/24/2005 0743 Davis & Floyd, Inc. I PO Drawer 428 I Greenwood. SC 29648 I 816 E. Durst Avenue I Greenwood, SC 2%49 I (8(l4) :229-4413 ] Fax (864) 229-7119 I LABORATORY ANALYSIS REPORT I I NC Certijica1ion Number: 25 I Client TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 I Contact Pem Carter Page 18 of 88 Report ID: AC1040 Client ID: P-58 Sample ID L05022007-01 Date collected: 02/17/2005 1820 I Matrix GW/ChemW Date Received 02/18/2005 Parameter Result Qual RDL Units Analyst Date Time I Volatile Organ_ics SW846 8260B 1,1,1-TRICHLOROETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544 I 1,1,2,2-TETRACHLOROETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544 1,1,2-TRICHLOROETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544 1,1-DICHLOROETHANE < 0. 0010 0.0010 mg/1 PAP 02/21/2005 1544 1, 1-DI,CHLOROETHENE < 0. 0010 0.0010 mg/1 PAP 02/21/2005 1544 I 1,2-DICHLOROETHANE < 0.0010 0 .0010 mg/1 PAP 02/21/2005 1544 1,2-DICHLOROPROPANE < 0.0010 0 . 0010 mg/1 PAP 02/21/2 DOS 1544 2-BUTANONE < 0.0050 o.ooso mg/1 PAP 02/21/2005 1544 I 2-HEXANONE < 0.0050 0.0050 mg/1 PAP 02/21/2005 1544 4-METHYL-2-PENTANONE < 0.0050 0.0050 mg/1 PAP 02/21/2005 1544 ACETONE 0.0091 0.0050 mg/1 PAP 02/21/2005 1544 BENZENE < o. 0010 0.0010 mg/1 PAP 02/21/2005 1544 I BROMODICHLOROMETHANE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1544 BROMOFORM < 0. 0010 0.0010 mg/1 PAP 02/21/2005 1544 BROMOMETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544 CARBON DISULFIDE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544 I CARBON TETRACHLORIDE < 0.0010 0. 0010 mg/1 PAP 02/21/200S 1S44 CHLOROBENZENE < o. 0010 0. 0010 mg/1 PAP 02/21/2005 1544 CHLOROETHANE < o. 0010 0.0010 mg/1 PAP 02/21/2005 1544 CHLOROFORM < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544 I CHLOROMETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544 CIS-1,2-DICHLOROETHENE < 0. 0010 0.0010 mg/1 PAP 02/21/2005 1544 CIS-1,3-DICHLOROPROPENE < 0. 0010 0. 0010 mg/1 PAP 02/21/200S 1544 I OIBROMOCHLOROMETHANE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1544 ETHYLBENZENE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544 METHYLENE CHLORIDE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544 STYRENE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544 I TETRACHLOROETHENE < 0:0010 0.0010 mg/1 PAP 02/21/2005 1544 TOLUENE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544 TRANS-1,2-DICHLOROETHENE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1544 TRANS-1,3-DICHLOROPROPENE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1544 I TRICHLOROETHENE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1544 VINYL ACETATE < 0 . 0010 0.0010 mg/1 PAP 02/21/2005 1544 VINYL CHLORIDE < 0 . 0010 0.0010 mg/1 PAP 02/21/2005 1544 I XYLENE {TOTAL) < 0 .0020 0.0020 mg/1 PAP 02/21/2005 1544 I D;wis & Floyd, Inc. I PO Dr<1wer 428 I Creenwood, SC 29648 I 81 fi E. Durst Avenue I Greenwood, SC 29649 I (864) 229-4413 I F.Jx (f\64) 229-71 19 I I I D~IS FL ~YD LABORATORY ANALYSIS REPORT I NC Cenification Number: 25 I Client TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD I HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Contact Fem Carter Page 19 of 88 Report ID: AC1040 I Client ID: l'-55 sample ID L05022007-02 Date Collected: 02/18/2005 1355 Matrix GW/ChemW Date Received 02/18/2005 I Parameter Result Qual RDL Units Analyst Date Time Semi volatile Organics I SW845 8270C 1,2,4-TRICHLOROBENZENE < 0.010 o. 010 mg/1 JRN 03/01/2005 1845 1,2-DICHLOROBENZENE < 0.010 o. 010 mg/1 JRN 03/01/2005 1845 I 1,3-DICHLOROBENZENE < 0.010 0 .010 mg/1 JRN 03/01/2005 1845 1,4-DICHµJROBENZENE < 0.010 0.010 mg/1 JRN 03/01/2005 1845 2, 4, 5-.TRICHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/01/2005 1845 2,4,6-TRICHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/01/2005 1845 I 2,4-DICHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/01/2005 1845 2,4-DIMETHYLPHENOL < 0.010 0.010 mg/1 JRN 03/01/2005 1845 2,4-DINITROPHENOL < 0.025 0.025 mg/1 JRN 03/01/2005 1845 2,4-DINITROTOLUENE < 0.010 0.010 mg/1 JRN 03/01/2005 1845 I 2,6-DINITROTOLUENE < 0. 010 0.010 mg/1 JRN 03/01/2005 1845 2-CHLORONAPHTHALENE < 0.010 0.010 mg/1 JRN 03/01/2005 1845 2 -CHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/01/2005 1845 I 2-METHYL-4,6-DINITROPHENOL < 0.025 0.025 mg/1 JRN 03/01/2005 1845 2-METHYLNAPHTHALENE 0.074 0.010 mg/1 JRN 03/01/2005 1845 2-METHYLPHENOL < 0.010 0.010 mg/1 JRN 03/01/2005 1845 2-NITROANILINE < 0.010 0.010 mg/1 JRN 03/01/2005 1845 I 2-NITROPHENOL < 0 010 0.010 mg/1 JRN 03/01/2005 1845 3,3'-DICHLOROBENZIDINE < 0.010 0.010 mg/1 JRN 03/01/2005 1845 3-NITROANILINE < 0.010 0.010 mg/1 JRN 03/01/2005 1845 4-BROMOPHENYL PHENYL ETHER < 0.010 0.010 mg/1 JRN 03/01/2005 1845 I 4-CHLOR0-3-METHYLPHENOL < 0.010 0.010 mg/1 JRN 03/01/2005 1845 4 -CHLOROANI LINE < 0.010 0.010 mg/1 JRN 03/01/2005 1845 4-CHLOROPHENYL PHENYL ETHER < 0.010 0.010 mg/1 JRN 03/01/2005 1845 I 4-METHYLPHENOL < 0.010 0.010 mg/1 JRN 03/01/2005 1845 4-NITROANILINE < 0.010 0.010 mg/1 JRN 03/01/2005 1845 4-NITROPHENOL < 0.025 0. 025 mg/1 JRN 03/01/2005 1845 ACENAPHTHENE < ().010 0.010 mg/1 JRN 03/01/2005 1845 I ACENAPHTHYLENE < 0.010 0.010 mg/1 JRN 03/01/2005 1845 ANTHRACENE < 0.010 0.010 mg/1 JRN 03/01/2005 1845 BENZO(A)ANTHRACENE < 0.010 0.010 mg/1 JRN 03/01/2005 1845 BENZO(A)PYRENE < 0. 010 0.010 mg/1 JRN 03/01/2005 1845 I BENZO(B)FLUORANTHENE < 0.010 0.010 mg/1 JRN 03/01/2005 1845 BENZO(G,H,I)PERYLENE < 0.010 0.010 mg/1 JRN 03/01/2005 1845 BENZO(K)FLUORANTHENE < 0.010 0. 010 mg/1 JRN 03/01/2005 1845 BENZOIC ACID < 0.050 0.050 mg/1 JRN 03/01/2005 1845 I BENZYL ALCOHOL < 0. 010 0. 010 mg/1 JRN 03/01/2005 1845 BIS(2-CHLOROETH0XY)METHANE < 0.010 0. 010 mg/1 JRN 03/01/2005 1845 BIS(2-CHLOROETHYL)ETHER < o. 010 0.010 mg/1 JRN 03/01/2005 1845 I BIS(2-CHLOROISOPROPYL)ETHER < 0.010 0.010 mg/1 JRN 03/01/2005 1845 Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2964H I s 10 E. Durst Avenue I Creenwood. SC 29649 I (86-1) 229-4413 I Fax (864) 229-7119 I 011s I FL '"'YD LABORATORY ANALYSIS REPORT I NC Cenijication Number: 25 Client TICONA,LLC Project Number, I 61621.01 2525 BLACKSBURG ROAD HWY 198 I I SHELBY, NC 28152 Report Date April 18, 2005 Contact Pem Carter Page 20 of 88 Report ID: AC1040 Client ID: F-55 Sample ID L05022007-02 I Date Collected: 02/18/2005 1355 Matrix GW/ChemW Date Received 02/18/2005 Parameter Result Qual RDL units Analyst Date Time I BIS(2-ETHYLHEXYL)PHTHALATE ' 0.010 0.010 mg/1 JRN 03/01/2005 1845 BUTYL BENZYL PHTHALATE ' 0. 010 0.010 mg/1 JRN 03/01/2005 1845 I CHRYSENE ' 0 .010 0.010 mg/1 JRN 03/01/2005 1845 DI -N-BUTYL PHTHALATE ' 0 .010 0.010 mg/1 JRN 03/01/2005 1845 DI-N-OCTYL PHTHALATE ' 0 .010 0.010 mg/1 JRN 03/01/2005 1845 I DIBENZ{A,H)ANTHRACENE ' 0 .010 0. 010 mg/1 JRN OJ/01/2005 1845 DIBENZOFURAN 0. 027 0.010 mg/1 JRN 03/01/2005 1845 DIETHYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/01/2005 1845 DIMETHYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/01/2005 1845 I FLUORANTHENE ' 0.010 0 .010 mg/1 JRN 03/01/2005 1845 FLUORENE ' 0.010 0 .010 mg/1 JRN 03/01/2005 1845 HEXACHLOROBENZENE ' 0.010 0 .010 mg/1 JRN 03/01/2005 1845 HEXACHLOROBUTADIENE ' 0.010 0 .010 mg/1 JRN 03/01/2005 1845 I HEXACHLOROCYCLOPENTADIENE ' 0.010 0. 010 mg/1 JRN 03/01/2005 1845 HEXACHLOROETHANE ' 0.010 O. 010 mg/1 JRN 03/01/2005 184 5 INDENO(l,2,3-CD)PYRENE ' 0.010 0 .010 mg/1 JRN 03/01/2005 1845 I ISOPHORONE ' 0.010 0 .010 mg/1 JRN 03/01/2005 1845 N-NITROSODI-N-PROPYLAMINE ' 0.010 0 .010 mg/1 JRN 03/01/2005 1845 N-NITROSOOIPHENYLAMINE ' 0.010 0. 010 mg/1 JRN 03/01/2005 184 5 NAPHTHALENE ' 0.010 o. 010 mg/1 JRN 03/01/2005 1845 I NITROBENZENE ' 0 .010 0 .010 mg/1 JRN 03/01/2005 1845 PENTACHLOROPHENOL ' 0 .025 0.025 mg/1 JRN 03/01/2005 1845 PHENANTHRENE ' 0 .010 0.010 mg/1 JRN 03/01/2005 1845 PHENOL 0.26 0.10 mg/1 JRN 03/02/2005 1256 I PYRENE ' 0.010 0.010 mg/1 JRN 03/01/2005 1845 SW846 8270C DOWTHERM 1, l' -Bl PHENYL 20.8 10.0 mg/1 JRN 03/01/2005 1806 I BIPHENYL ETHER 62.7 10.0 mg/1 JRN 03/01/2005 1806 Volatile Organics SW846 8260B I 1,1,1-TRICHLOROETHANE ' 0 .0030 X 0.0030 mg/1 PAP 02/21/2005 162 0 1,1,2,2-TETRACHLOROETHANE ' 0 .0030 X 0 . 0030 mg/1 PAP 02/21/2005 1620 1,1,2-TRICHLOROETHANE ' 0 .0030 X 0 .0030 mg/1 PAP 02/21/2005 1620 1,1-DICHLOROETIWfE ' 0.0030 X 0 .0030 mg/1 PAP 02/21/2005 1620 I 1,1-DICHLOROETHENE ' 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620 1,2-DICHLOROETHANE ' 0 .0030 X 0.0030 mg/1 PAP 02/21/2005 1620 1,2-DICHLOROPROPANE ' o. 0030 X 0.0030 mg/1 PAP 02/21/2005 1620 I 2-BUTANONE ' 0.015 X 0.015 mg/1 PAP 02/21/2005 1620 2-HEXANONE ' 0.015 X 0.015 mg/1 PAP 02/21/2005 1620 4-METHYL-2-PENTANONE ' 0 .015 X 0 .015 mg/1 PAP 02/21/2005 1620 ACETONE ' 0 .015 X 0 .015 mg/1 PAP 02/21/2005 1620 I D;ivi~ & Floyrl, Inc. I PO Drawer 428 I Creenwoorl, SC 2%48 I s Ir, E. Durst Avenue I Greenwood, SC 2964~! / (8(i4) 229-4413 I Fax (HCi4) n9-7 t 19 I I I I I I I I I I I I I I I I I I I DAYIS FLOYD Client Contact Client Matrix Parameter BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOR0}3ENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE ID: CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) Prep Procedure Analytical Prep Procedures1 OOWTHERM 8270 SVOC PREP LABORATORY ANALYSIS REPORT NC Cenificarion Number: 25 TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Pem Carter Page 21 of 88 Report ID: AC1040 F-55 Sample ID L05022007-02 Date Collected: 02/18/2005 1355 GW/ChemW Date Received 02/18/2005 Result Qual RDL Units Analyst Date Time 0.051 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0 0030 X 0.0030 mg/1 PAP 02/21/2005 1620 < o. 0030 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0. 0030 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620 0. 014 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620 0.0057 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0 0030 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620 < 0.0030 X 0 . 0030 mg/1 PAP 02/21/2005 1620 < 0.0060 X 0.0060 mg/1 PAP 02/21/2005 1620 Method Analyst Prep Date SWB46 3500B DBC 02/22/2005 0B00 SWB46 3510C DBC 02/22/2005 0B00 Davis & Floyd. Inc. I PO Drawer 428 I Creemvood, SC 29648 I H 16 E. Durst Avenue I Greenwood. SC 2%49 I (864) 2.29-4413 I Fax (864) n9-7119 DAYIS FLtrYD LABORATORY ANALYSIS REPORT NC Certification Number: 25 Client TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Contact Pem Carter Page 22 of 88 Report ID: AC1040 Client ID: CC-33 Sample ID L05022007-03 Date Collected: 02/18/2005 1019 Matrix : GW/Chemw Date Received 02/18/2005 Parameter Result Qual RDL Units Analyst Date Time Volatile Organics SW845 8260B 1,1,1-TRICHLOROETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602 1,1,2,2-TETRACHLOROETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602 1,1,2-TRICHLOROETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602 1, 1-DICHLOROETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602 1, 1-DI,CHLOROETHENE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602 1,2-DICHLOROETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602 1,2-DICHLOROPROPANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602 2-BUTANONE < 0.0050 0.0050 mg/1 PAP 02/21/2005 1602 2-HEXANONE < 0.0050 0.0050 mg/1 PAP 02/21/2005 1602 4-METHYL-2-PENTANONE < o.ooso 0.0050 mg/1 PAP 02/21/2005 1602 ACETONE < 0.0050 0.0050 mg/1 PAP 02/21/2005 1602 BENZENE < 0 0010 0.0010 mg/1 PAP 02/21/2005 1602 BROMODICHLOROMETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602 BROMOFORM < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602 BROMOMETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602 CARBON DISULFIDE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602 CARBON TETRACHLORIDE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602 CHLOROBENZENE 0.0019 0.0010 mg/1 PAP 02/21/2005 1602 CHLOROETHANE < o. 0010 0.0010 mg/1 PAP 02/21/2005 1602 CHLOROFORM < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602 CHLOROMETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602 CIS-1,2-DICHLOROETHENE 0.0022 0.0010 mg/1 PAP 02/21/2005 1602 CIS-1,3-DICHLOROPROPENE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1602 DIBROMOCHLOROMETHANE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1602 ETHYLBENZENE < 0 0010 0.0010 mg/1 PAP 02/21/2005 1602 METHYLENE CHLORIDE < 0 0010 0.0010 mg/1 PAP 02/21/2005 1602 STYRENE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602 TETRACHLOROETHENE < 0:0010 0. 0010 mg/1 PAP 02/21/2005 1602 TOLUENE < 0 . 0010 0.0010 mg/1 PAP 02/21/2005 1602 TRANS-1,2-DICHLOROETHENE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1602 TRANS-1,3-DICHLOROPROPENE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1602 TRICHLOROETHENE < 0 0010 0.0010 mg/1 PAP 02/21/2005 1602 VINYL ACETATE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1602 VINYL CHLORIDE < 0 0010 o. 0010 mg/1 PAP 02/21/2005 1602 XYLENE {TOTAL) < 0 .0020 0.0020 mg/1 PAP 02/21/2005 1602 Davis & Floyd, Inc. 1 · PO Drawer ..t28 I Greenwood, SC 29648 I 816 E. Durst Avenue / Greenwood, SC ~9649 I (864) 229-4413 I Fax (1:164) 229-71 l 9 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I D~IS FLOYD Client Contact Client Matrix Parameter Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE ID: 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICHLOROETHANE 1,1-DICHLOROETHANE l, l-□r.cin.oROETHENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 2-BUTANONE 2-HEXANONE 4-METHYL-2-PENTANONE ACETONE BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) LABORATORY ANALYSIS REPORT NC Certification Number: 25 TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Fem carter Page 23 of 88 Report ID: AC1040 TRIP BLANX-2 Sample ID L05022007-04 Date Collected: 02/03/2005 1450 GW/Chemw Date Received 02/18/2005 Result Qual RDL Units Analyst Date Time < 0 0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0. 0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0 0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0 0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0 0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0.0010 0.0010 . mg/1 PAP 02/21/2005 1204 < 0.0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0 0050 0.0050 mg/1 PAP 02/21/2005 1204 < 0 .0050 0.0050 mg/1 PAP 02/21/2005 1204 < 0 .0050 0.0050 mg/1 PAP 02/21/2005 1204 < 0 0050 0.0050 mg/1 PAP 02/21/2005 1204 < 0 0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0. 0010 0.0010 mg/1 PAP 02/21/2005 1204 < o. 0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0.0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0 0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0 0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0 0010 0 0010 mg/1 PAP 02/21/2005 1204 < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0 0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0 .0010 0. ◊-010 mg/1 PAP 02/21/2005 1204 < 0.0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0 0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0.0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0.0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0.0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0.0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0.0010 · 0.0010 mg/1 PAP 02/21/2005 1204 < 0 0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0.0010 0 .0010 mg/1 PAP 02/21/2005 1204 < 0.0010 0.0010 mg/1 PAP 02/21/2005 12 04 < 0.0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0.0010 0.0010 mg/1 PAP 02/21/2005 1204 < 0.0010 0 0010 mg/1 PAP 02/21/2005 1204 < 0.0020 0.0020 mg/1 PAP 02/21/2005 1204 D.ivis K Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC ~9649 I (864) 229-4413 I Fax (864) 229-7119 I 011s I FL ~~YD LABORATORY ANALYSIS REPORT I NC Certification Number: 25 Client TICONA,LLC Project Number: I 61621.01 2525 BLACKSBURG ROAD HWY 198 I SHELBY, NC 28152 Report Date April 18, 2005 Contact Pem Carter Page 24 of 88 Report ID: AC1040 Client ID: PEW-1 Sample ID L05022303-01 I Date Collected: 02/22/2005 1343 Matrix GW/ChemW Date Received 02/22/2005 Para.meter Result Qual RDL Units Analyst Date Time I Semi volatile Organics SW846 8270C I 1,2,4-TRICHLOROBENZENE < 0.010 0. 010 mg/1 JRN 03/03/2005 1238 1,2-DICHLOROBENZENE < 0.010 0.010 mg/1 JRN 03/03/2005 1238 1,3-DICHLOROBENZENE < 0.010 0. 010 mg/1 JRN 03/03/2005 1238 I 1,4-DICHLOROBENZENE < 0.010 0. 010 mg/1 JRN 03/03/2005 1238 2,4,S~TRICHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1238 2,4,6-TRICHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1238 2,4-DICHLOROPHENOL < 0 010 0.010 mg/1 JRN 03/03/2005 1238 I 2,4-DIMETHYLPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1238 2,4-DINITROPHENOL < 0 .025 0.025 mg/1 JRN 03/03/2005 1238 2,4-DINITROTOLUENE < o. 010 0.010 mg/1 JRN 03/03/2005 123 8 2,6-DINITROTOLUENE < 0. 010 0.010 mg/1 JRN 03/03/2005 1238 I 2 -CHLORONAPHTHALENE < 0.010 0. 010 mg/1 JRN 03/03/2005 1238 2 -CHLOROPHENOL < 0.010 0. 010 mg/1 JRN 03/03/2005 1238 2-METHYL-4,6-DINITROPHENOL < 0.025 0. 025 mg/1 JRN 03/03/2005 1238 I 2-METHYLNAPHTHALENE < 0. 010 0. 010 mg/1 JRN 03/03/2005 1238 2-METHYLPHENOL < 0. 010 0. 010 mg/1 JRN 03/03/2005 1238 2-NITROANILINE < 0.010 0 010 mg/1 JRN 03/03/2005 1238 2-NITROPHENOL < 0.010 0 010 mg/1 JRN 03/03/2005 1238 I 3,3'-DICHLOROBENZIDINE < 0 010 0.010 mg/1 JRN 03/03/2005 1238 3-NITROANILINE < 0.010 0. 010 mg/1 JRN 03/03/2005 1238 4-BROMOPHENYL PHENYL ETHER < o. 010 0.010 mg/1 JRN 03/03/2005 123 8 4-CHLOR0-3-METHYLPHENOL < o. 010 0.010 mg/1 JRN 03/03/2005 1238 I 4-CHLOROANILINE < 0 010 0.010 mg/1 JRN 03/03/2005 1238 4-CHLOROPHENYL PHENYL ETHER < 0 010 0.010 mg/1 JRN 03/03/2005 1238 4-METHYLPHENOL < 0 010 0.010 mg/1 JRN 03/03/2005 1238 I 4-NITROANILINE < o. 010 0.010 mg/1 JRN 03/03/2005 1238 4-NITROPHENOL < 0.025 0.025 mg/1 JRN 03/03/2005 1238 ACENAPHTHENE < 0.010 0. 010 mg/1 JRN 03/03/2005 1238 ACENAPHTHYLENE < 0.010 0.010 mg/1 JRN 03/03/2005 1238 I ANTHRACENE < 0 010 0.010 mg/1 JRN 03/03/2005 1238 BENZO(A)ANTHRACENE < 0 010 0. 010 mg/1 JRN 03/03/2005 1238 BENZO(A)PYRENE < 0. 010 0.010 mg/1 JRN 03/03/2005 1238 BENZO(B)FLUORANTHENE < 0.010 0.010 mg/1 JRN 03/03/2005 1238 I BENZO(G,H,I)PERYLENE < 0.010 0.010 mg/1 JRN 03/03/2005 1238 BENZO(K)FLUORANTHENE < 0.010 0.010 mg/1 JRN 03/03/2005 1238 BENZOIC ACID < 0.050 0 .050 mg/1 JRN 03/03/2005 1238 I BENZYL ALCOHOL < 0.010 0 .010 mg/1 JRN 03/03/2005 1238 BIS(2-CHLOROETHOXY)METHANE < 0.010 0. 010 mg/1 JRN 03/03/2005 1238 BIS(2-CHLOROETHYL)ETHER < 0. 010 0.010 mg/1 JRN 03/03/2005 1238 BIS(2-CHLOROISOPROPYL)ETHER < 0.010 0 010 mg/1 JRN 03/03/2005 1238 I Davis & Floyd, Inc. I PO Drawer 428 I Greemvoud, SC 2964R I 816 E. Durst Avenue ! Creenwood, SC 29649 I (864) 229-4413 I Fax (8()4) 229-71 I~ I I D~IS LABORATORY ANALYSIS REPORT FLMD I NC Cenification Number: 25 I Client TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD I HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Contact Pem Carter Page 25 of 88 Report ID: AC1040 I Client ID: PBW-1 Sample ID L05022303-01 Date Collected: 02/22/2005 1343 Matrix GW/ChemW Date Received 02/22/2005 I Parameter Result Qual RDL units Analyst Date Time BIS(2-ETHYLHEXYL)PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238 I BUTYL BENZYL PHTHALATE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1238 CHRYSENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238 DI-N-BUTYL PHTHALATE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1238 DI-N-OCTYL PHTHALATE ' 0. 010 0. 010 mg/1 JRN 03/03/2005 1238 I DIBENZ{A,H)ANTHRACENE ' 0.010 0 010 mg/1 JRN 03/03/2005 1238 DIBEN2;0FURAN ' 0.010 0 .010 mg/1 JRN 03/03/2005 1238 DIETHYL PHTHALATE ' 0. 010 0.010 mg/1 JRN 03/03/2005 1238 I DIMETHYL PHTHALATE ' 0. 010 0.010 mg/1 JRN 03/03/2005 1238 FLUORANTHENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238 FLUORENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1238 HEXACHLOROBENZENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238 I HEXACHLOROBUTADIENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238 HEXACHLOROCYCLOPENTADIENE ' 0. 010 0. 010 mg/1 JRN 03/03/2005 1238 HEXACHLOROETHANE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238 INDENO(l,2,3-CD)PYRENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238 I ISOPHORONE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238 N-NITROSODI-N-PROPYLAMINE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238 N-NITROSODIPHENYLAMINE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238 I NAPHTHALENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238 NITROBENZENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238 PENTACHLOROPHENOL ' 0.025 0. 025 mg/1 JRN 03/03/2005 1238 PHENANTHRENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238 I PHENOL ' 0.010 0.010 mg/1 JRN 03/03/2005 1238 PYRENE ' 0 .010 0.010 mg/1 JRN 03/03/2005 1238 SW846 8270C DOWTHERM 1, l' -BI PHENYL ' 0 010 0.010 mg/1 JRN 03/03/2005 1238 I BIPHENYL ETHER ' 0 .010 0.010 mg/1 JRN 03/03/2005 1238 Volatile Organics I SWB46 8260B 1,1,1-TRICHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0856 1,1,2,2-TETRACHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0856 1,1,2-TRICHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0856 I 1,1-DICHLOROETHANE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0856 1,1-DICHLOROETHENE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0856 1,2-DICHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0856 1,2-DICHLOROPROPANE ' 0.0010 0. 0010 mg/1 PAP 02/24/2005 0856 I 2-BUTANONE ' o.ooso 0.0050 mg/1 PAP 02/24/2005 0856 2-HEXANONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0856 4-METHYL-2 PENTANONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0856 I ACETONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0856 Duvis & Floyd, Inc. I PO Drawer 428 I Greenwood. SC 296413 I 816 E. Durst Avenue I Creenwood, SC 29649 I (864) 229-4413 I Fa, (8641229-7119 DAYIS FLbYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter Client ID: PEW-l Matrix Parlllrleter BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLORO_BENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) Prep Procedure Analytical Prep Proceduresi OOWTHERM 8270 SVOC PREP GW/ChemW < < < < < < < < < < < < < < < < < < < < < Method SW846 3500B SW846 3510C Result Qual 0. 0010 0 .0010 0 .0010 0 .0010 0.0010 0.0010 0.0010 0.0010 0.0016 0.0010 0.0012. 0.0010 0.0010 0 .0010 0. 0010 0.0010 0.0010 0 . 0010 o. 0010 0 .0010 0.0055 0.0010 0.0010 0.0020 Analyst DBC DBC NC Cenification Number: 25 Project Number: 61621.01 Report Date Page 26 of 8B April 18, 2005 Report ID: AC1040 Sample ID L05022303-01 Date Collected: 02/22/2005 1343 Date Received 02/22/2005 RDL Units 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0 . 0010 mg/1 o . 0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0. 002 0 mg/1 Prep Date 02/28/2005 0800 02/28/2005 0800 Analyst PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP Date 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 Time 0856 0856 0856 0856 0856 0856 0856 0856 0856 0856 0856 0856 0856 0856 0856 0856 0856 0856 0856 0856 0856 0856 0856 0856 D,ivis & Floyrl, Inc. / PO Drawer 428 I Greenwood, SC 2%48 I 816 E. Durst Avenue I Greenwood, SC 29649 I (H64) 229-4413 I Fax (864) 229-7119 I I I I I I I I I I I I I I I I I I I I I D~S LABORATORY ANALYSIS REPORT FL D I NC Certification Number: 25 I Client TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD I HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Contact Pem Carter Page 27 of 88 Report ID: AC1040 I Client ID: PEW-3 Sample ID L05022303-02 Date Collected: 02/22/2005 1453 Matrix GW/ChemW Date Received 02/22/2005 I Parameter Result Qual RDL Units Analyst Date Time Semi volatile Organics I SWB46 8270C 1,2,4-TRICHLOROBENZENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1515 1,2-DICHLOROBENZENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1515 1,3-DICHLOROBENZENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1515 I 1,4-DICHLOROBENZENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1515 2, 4, 5-,TRICHLOROPHENOL ' 0.010 0.010 mg/1 JRN 03/03/2005 1515 2,4,6-TRICHLOROPHENOL ' 0.010 0.010 mg/1 JRN 03/03/2005 1515 I 2,4-DICHLOROPHENOL ' 0.010 0. 010 mg/1 JRN 03/03/2005 1515 2,4-DIMETHYLPHENOL ' 0.010 0.010 mg/1 JRN 03/03/2005 1515 2,4-DINITROPHENOL ' 0. 025 0.025 mg/1 JRN 03/03/2005 1515 2,4-DINITROTOLUENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1515 I 2,6-DINITROTOLUENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1515 2-CHLORONAPHTHALENE ' 0. 010 0.010 mg/1 JRN 03/03/2005 1515 2-CHLOROPHENOL ' 0.010 0.010 mg/1 JRN 03/03/2005 1515 2-METHYL-4,6-DINITROPHENOL ' 0. 025 0.025 mg/1 JRN 03/03/2005 1515 I 2-METHYLNAPHTHALENE ' o. 010 0.010 mg/1 JRN 03/03/2005 1515 2 -METHYLPHENOL ' 0 .010 0.010 mg/1 JRN 03/03/2005 1515 2-NITROANILINE ' 0.010 0.010 mg/1 JRN 03/03/2005 1515 I 2-NITROPHENOL ' 0 010 0.010 mg/1 JRN 03/03/2005 1515 3,3'-DICHLOROBENZIDINE ' 0. 010 0.010 mg/1 JRN 03/03/2005 1515 3-NITROANILINE ' 0. 010 0.010 mg/1 JRN 03/03/2005 1515 4-BROMOPHENYL PHENYL ETHER ' 0. 010 0.010 mg/1 JRN 03/03/2005 1515 I 4-CHLOR0-3-METHYLPHENOL ' 0 .010 0. 010 mg/1 JRN 03/03/2005 1515 4-CHLOROANILINE ' 0 010 0.010 mg/1 JRN 03/03/2005 1515 4-CHLOROPHENYL PHENYL ETHER ' 0.010 0.010 mg/1 JRN 03/03/2005 1515 4-METHYLPHENOL ' 0. 010 0 .010 mg/1 JRN 03/03/2005 1515 I 4-NITROANILINE ' 0. 010 0.010 mg/1 JRN 03/03/2005 1515 4-NITROPHENOL ' 0 .025 0.025 mg/1 JRN 03/03/2005 1515 ACENAPHTHENE ' 0. 010 0.010 mg/1 JRN 03/03/2005 1515 I ACENAPHTHYLENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1515 ANTHRACENE ' 0 010 0.010 mg/1 JRN 03/03/2005 1515 BENZO(A)ANTHRACENE ' 0 010 0.010 mg/1 JRN 03/03/2005 1515 BENZO (A) PYRENE ' 0.010 0.010 mg/1 JRN 03/03/2005 15_15 I BENZO(B)FLUORANTHENE ' 0 010 0.010 mg/1 JRN 03/03/2005 1515 BENZO(G,H,I)PERYLENE ' 0 .010 0.010 mg/1 JRN 03/03/2005 1515 BENZO(K)FLUORANTHENE ' 0 010 0. 010 mg/1 JRN 03/03/2005 1515 BENZOIC ACID ' 0. 050 o.oso mg/1 JRN 03/03/2005 1515 I BENZYL ALCOHOL ' 0 010 0. 010 mg/1 JRN 03/03/2005 1515 BIS(2-CHLOROETHOXY)METHANE ' 0 010 0.010 mg/1 JRN 03/03/2005 1515 BIS(2-CHLOROETHYL)ETHER ' 0.010 0.010 mg/1 JRN 03/03/2005 1515 I 8IS(2-CHLOROISOPROPYL)ETHER ' 0.010 0.010 mg/1 JRN 03/03/2005 1515 D.ivis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue l Greenwood, SC 29649 I (BG4) 229-44 U I Fax (864) 229-711 Y DAVIS FL6YD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter Client ID: PEW-3 Matrix Para.meter BIS(2-ETHYLHEXYL)PHTHALATE BUTYL BENZYL PHTHALATE CHRYSENE DI·N-BUTYL PHTHALATE DI-N-OCTYL PHTHALATE DIBENZ(A,H)ANTHRACENE DIBENZOFURAN DIETHYL PHTHALATE DIMETHYL PHTHALATE FLUORANTHENE FLUORENE HEXACHLOROBENZENE HEXACHLOROBUTADIENE HEXACHLOROCYCLOPENTADIENE HEXACHLOROETHANE INDENO(l,2,3-CD)PYRENE ISOPHORONE N-NITROSODI-N-PROPYLAMINE N-NITROSODIPHENYLAMINE NAPHTHALENE NITROBENZENE PENTACHLOROPHENOL PHENANTHRENE PHENOL PYRENE SW846 8270C DOWTHERM 1, 1' -BI PHENYL BIPHENYL ETHER Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICHLOROETHANE 1,1-DICHLOROETHANE 1,1-DICHLOROETHENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 2-BUTANONE 2-HEXANONE 4-METHYL-2-PENTANONE ACETONE GW/ChemW ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' Result Qual 0.010 o. 010 0 .010 0 .010 0. 010 0.010 0. 010 0.010 0. 010 0.010 0.010 0.010 0.010 0. 010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0. 025 0. 010 0. 010 0.010 0.27 0.86 0.0010 0.0010 0.0010 0.0010 0 .0010 0 .0010 0.0010 0.0050 o.ooso 0.0050 0.0050 NC Certification Number: 25 Project Number: 61621.01 Report Date Page 28 of 88 Sample ID Date Collected: Date Received RDL Units 0.010 mg/1 0.010 mg/1 0 .010 mg/1 0. 010 mg/1 0. 010 mg/1 0. 010 mg/1 0. 010 mg/1 o. 010 mg/1 0 .010 mg/1 0.010 mg/1 0. 010 mg/1 0. 010 mg/1 0.010 mg/1 0. 010 mg/1 0. 010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0. 010 mg/1 0. 010 mg/1 0 .010 mg/1 0.025 mg/1 0.010 mg/1 0 .010 mg/1 0 .010 mg/1 0. 040 mg/1 0.10 rng/1 0.0010 rng/1 0.0010 mg/1 0.0010 rng/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0 .0010 mg/1 0 . 0050 mg/1 0.0050 mg/1 0.0050 rng/1 0.0050 mg/1 April 18, 2005 Report ID: AC1040 L05022303-02 02/22/2005 1453 02/22/2005 Analyst JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP Date 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 03/03/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 Time 1515 1515 1515 1515 1515 1515 1515 1515 1515 1515 1515 1515 1515 1515 1515 1515 1515 1515 1515 1515 1515 1515 1515 1515 1515 1438 1756 0915 0915 0915 0915 0915 0915 0915 0915 0915 0915 0915 Davis & Floyd, Inc. ! PO Drawer 428 I Greenwood, SC 29648 I fl 1 fi F.. Durst Avenue I Greenwood,. SC 29649 I (864) 2'..!~l-4413 I Fax (864) 229-71 19 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I D~IS FLOYD LABORATORY ANALYSIS REPORT Client TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Contact Pem Carter Client ID: PBW-3 Matrix : GW/ChemW Parameter BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLORQBENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) Prep Procedure Analytical Prep Procedures: DOWTHERM 8270 SVOC PREP ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' Method SW846 3500B SW846 3510C Result Qual 0.0010 0.0010 0.0010 0 0010 0 .0010 0 0010 0 . 0010 0.0010 0.0010 0.0010 0.0010 0 0010 0 0010 0 .0010 0. 0010 0. 0010 0. 0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0020 Analyst DBC DBC NC Certification Number: 25 Project Number: Report Date Page 29 of 88 Sample ID Date Collected: Date Received RDL Units 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0 .0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0. 002 0 mg/1 Prep Date 02/28/2005 0800 02/28/2005 0800 61621.01 April 18, 2005 Report ID: AC1040 LOS022303-02 02/22/2005 1453 02/22/2005 Analyst Date PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 PAP 02/24/2005 Time 0915 0915 0915 0915 0915 0915 0915 0915 0915 0915 0915 0915 0915 0915 0915 0915 0915 0915 0915 0915 0915 0915 0915 0915 Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2964H I 816 E. Durst Avenue I Grcemvoorl, SC 2%49 I (864) 229-44.13 I Fax (864) 229-7119 I D\VIS I FLOYD LABORATORY ANALYSIS REPORT I NC Cenijicarion Number: 25 Client TICONA,LLC Project Number: I 61621. 01 2525 BLACKSBURG ROAD I HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Contact Pem Carter Page 30 of 88 Report ID: AC1040 Client IO: PEW-4 Sample ID L05022303-03 I Date Collected: 02/22/2005 1443 Matrix : GW/ChemW Date Received 02/22/2005 Parameter Result Qual RDL Units Analyst Date Time I semi volatile eJ:rganics SW846 8270C I 1,2,4-TRICHLOROBENZENE < 0 .010 0.010 mg/1 JRN 03/03/2005 1557 1,2-DICHLOROBENZENE < 0. 010 0.010 mg/1 JRN 03/03/200S 1557 1,3-DICHLOROBENZENE < 0.010 0.010 mg/1 JRN 03/03/2005 1557 I 1,4-DICHLOROBENZENE < 0.010 0. 010 mg/1 JRN 03/03/2005 1557 2, 4, 5-,TRICHLOROPHENOL < 0.010 0. 010 mg/1 JRN 03/03/2005 1557 2,4,6-TRICHLOROPHENOL < 0.010 0. 010 mg/1 JRN 03/03/2005 1557 2,4-DICHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1557 I 2,4-DIMETHYLPHENOL < 0.010 0. 010 mg/1 JRN 03/03/2005 1557 2, 4-DINITROPHENOL < 0.025 0.025 mg/1 JRN 03/03/2005 1557 2,4-DINITROTOLUENE < 0.010 0.010 mg/1 JRN 03/03/2005 1557 2,6-DINITROTOLUENE < 0. 010 0 .010 mg/1 JRN 03/03/2005 1557 I 2-CHLORONAPHTHALENE < 0.010 0 .010 mg/1 JRN 03/03/2005 1557 2 -CHLOROPHENOL < 0. 010 0.010 mg/1 JRN 03/03/2005 1557 2-METHYL-4,6-DINITROPHENOL < 0 .025 0.025 mg/1 JRN 03/03/2005 1557 I 2-METHYLNAPHTHALENE < 0. 010 0 .010 mg/1 JRN 03/03/2005 1557 2-METHYLPHENOL < 0. 010 0. 010 mg/1 JRN 03/03/2005 1557 2-NITROANILINE < 0 .010 o. 010 mg/1 JRN 03/03/2005 1S57 2-NITROPHENOL < 0.010 o. 010 mg/1 JRN 03/03/2005 1557 I 3,3'-DICHLOROBENZIDINE < 0 .010 0 .010 mg/1 JRN 03/03/2005 1557 3-NITROANILINE < 0 .010 0.010 mg/1 JRN 03/03/2005 1557 4-BROMOPHENYL PHENYL ETHER < 0. 010 0.010 mg/1 JRN 03/03/2005 1557 4-CHLOR0-3-METHYLPHENOL < 0. 010 0.010 mg/1 JRN 03/03/2005 1557 I 4-CHLOROANILINE < 0.010 0.010 mg/1 JRN 03/03/2005 1557 4-CHLOROPHENYL PHENYL ETHER < 0.010 0. 010 mg/1 JRN 03/03/2005 1557 4-METHYLPHENOL < 0.010 0. 010 mg/1 JRN 03/03/2005 1557 I 4-NITROANILINE < o. 010 0.010 mg/1 JRN 03/03/2005 1557 4-NITROPHENOL < 0.025 0. 025 mg/1 JRN 03/03/2005 1557 ACENAPHTHENE < 0. 010 o. 010 mg/1 JRN 03/03/2005 1557 ACENAPHTHYLENE < o. 010 0.010 mg/1 JRN 03/03/2005 1557 I ANTHRACENE < 0 .010 0. 010 mg/1 JRN 03/03/2005 1557 BENZO(A)ANTHRACENE < 0. 010 0.010 mg/1 JRN 03/03/2005 1557 BENZO(A)PYRENE < 0 .010 0.010 mg/1 JRN 03/03/2005 1557 BENZO(B)FLUORANTHENE < 0 .010 0. 010 mg/1 JRN 03/03/2005 1557 I BENZO(G,H,I)PERYLENE < 0.010 0. 010 mg/1 JRN 03/03/2005 1557 BENZO(K)FLUORANTHENE < o. 010 0.010 mg/1 JRN 03/03/2005 1557 BENZOIC ACID < 0. 050 0 .050 mg/1 JRN 03/03/2005 1557 I BENZYL ALCOHOL < 0 .010 0. 010 mg/1 JRN 03/03/2005 1557 BIS(2-CHLOROETHOXY)METHANE < 0 .010 0. 010 mg/1 JRN 03/03/2005 1557 BIS(2-CHLOROETHYL)ETHER < 0. 010 0.010 mg/1 JRN 03/03/2005 1557 BIS(2-CHLOROISOPROPYL)ETHER < 0. 010 0.010 mg/1 JRN 03/03/2005 1557 I D,wis & Floyd, Inc. I ro Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 2%49 I (8(,4) :229-4-1 I J I Fax (864) 22lJ-7 ! 19 I I 011s LABORATORY ANALYSIS REPORT FL 'YD I NC Certification Number: 25 I Client TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD I HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Contact Pem Carter Page 31 of 88 Report ID: AC1040 I Client ID: PBW-4 Sample ID L05022303-03 Date Collected, 02/22/2005 1443 Matrix GW/ChemW Date Received 02/22/2005 I Parameter Result Qual RDL units Analyst Date Time BIS{2-ETHYLHEXYL)PHTHALATE ' 0.010 0. 010 mg/i JRN 03/03/2005 1557 I BUTYL BENZYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557 CHRYSENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557 DI-N-BUTYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557 I D1-N-OCTYL PHTHALATE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1557 DIBENZ(~,H)ANTHRACENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557 DIBENZOFURAN ' 0.010 0.010 mg/1 JRN 03/03/2005 1557, DIETHYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557 I DIMETHYL PHTHALATE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1557 FLUORANTHENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1557 FLUORENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1557 HEXACHLOROBENZENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1557 I HEXACHLOROBlITADIENE ' 0.010 o. 010 mg/1 JRN 03/03/2005 1557 HEXACHLOROCYCLOPENTADIENE ' 0.010 0 010 mg/1 JRN 03/03/2005 1557 HEXACHLOROETHANE ' 0.010 o. 010 mg/1 JRN 03/03/2005 1557 I INDENO(l,2,3-CD)PYRENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1557 ISOPHORONE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557 N-NITROSODI-N-PROPYLAMINE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557 N-NITROSODIPHENYLAMINE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557 I NAPHTHALENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557 NITROBENZENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557 PENTACHLOROPHENOL ' 0.025 0.025 mg/1 JRN 03/03/2005 1557 PHENANTHRENE ' 0.010 0 .010 mg/1 JRN 03/03/2005 1557 I PHENOL ' 0.010 0. 010 mg/1 JRN 03/03/2005 1557 PYRENE ' 0.010 o. 010 mg/1 JRN 03/03/2005 1557 SWB46 8270C DOWTHERM I 1,1'-BIPHENYL ' 0.010 0 .010 mg/1 JRN 03/03/2005 1557 BIPHENYL ETHER 0. 026 0.010 mg/1 JRN 03/03/2005 1557 Volatile Organics I SW846 8260B 1,1,1-TRICHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0933 1,1,2,2-TETRACHLOROETHANE ' 0 0010 0.0010 mg/1 PAP 02/24/2005 0933 1,1,2-TRICHLOROETHANE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0933 I 1,1-DICHLOROETHANE ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 0933 1,1-DICHLOROETHBNE ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 0933 1,2-DICHLOROETHANE ' 0 0010 0.0010 mg/1 PAP 02/24/2005 0933 1,2-DICHLOROPROPANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0933 I 2-BUTANONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0933 2-HEXANONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0933 4-METHYL-2-PENTANONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0933 I ACETONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0933 Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2Yf>413 I 816 E. Durst AVt:!lllle I Greenwood, SC 2%49 I 1864) 229-4413 I Fox (864) 229-7119 Df\lIS FLOYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter Client ID: PEW-4 Matrix ; GW/Chemw Para.meter BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE OIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) Prep Procedure Analytical Prep Procedures, DOWTHERM 8270 SVOC PREP < < < < < < < < < < < < < < < < < < < < Method SW846 35008 SW846 3510C Result Qual 0.0026 0. 0010 0 .0010 0 .0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0056 0 .0010 0. 0010 0.0010 0. 0010 0 .0010 0 .0010 0. 0010 0.0010 0.0010 0.015 0.0010 0.0010 0.0020 Analyst DBC DBC NC Certification Number: 25 Project Number: 61621.01 Report Date Page 32 of 88 April 18, 2005 Report ID: AC1040 Sample ID L05022303-03 Date Collected: 02/22/2005 1443 Date Received 02/22/2005 RDL Units 0 .0010 mg/1 0. 0010 mg/1 0.0010 mg/1 0.0010 mg/1 0 .0010 mg/1 0 .0010 mg/1 0 .0010 mg/1 o. 0010 mg/1 0.0010 mg/1 0 .0010 mg/1 0. 0010 mg/1 0 .0010 mg/1 0. 0010 mg/1 0.0010 mg/1 0. 0010 mg/1 0 .0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0 .0010 mg/1 0. 0010 mg/1 0 .0010 mg/1 0.0010 mg/1 0.0020 mg/1 Prep Date 02/28/2005 0800 02/28/2005 0800 Analyst PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP Date 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 02/24/2005 Time 0933 0933 0933 0933 0933 0933 0933 0933 0933 093 3 0933 0933 0933 0933 0933 0933 0933 0933 0933 0933 0933 0933 0933 0933 Davis & Floyd, Inc. I PO Drawer 42B I Greenwood, SC 2%48 I 81 fi E. Durst 1\venut! I Greenwo(ld, SC 2%49 I (864) 229~44 lJ I Fax (864) 229-71 I 9 I I I I I I 11 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAVIS FL6YD LABORATORY ANALYSIS REPORT NC Certification Number: 25 Client TICONA,LLC Project Number: 61621. 01 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Contact Fem Carter Page 33 of 88 Report ID: AC1040 Client ID: DUP-4 Sample ID LOS022303-04 Date Collected: 02/22/2005 0000 Matrix GW/ChemW Date Received 02/22/2005 Parameter Result Oual RDL Units Analyst Date Time Semi volatile organics SW846 8270C 1,2,4-TRICHLOROBENZENE < 0 .010 0.010 mg/1 JRN 03/03/2005 1636 1,2-DICHLOROBENZENE < 0 .010 0. 010 mg/1 JRN 03/03/2005 1636 1,3-DICHLOROBENZENE < 0 .010 0. 010 mg/1 JRN 03/03/2005 1636 1,4-DIC~LOROBENZENE < 0 .010 0.010 mg/1 JRN 03/03/2005 1636 2, 4, S-:tRICHLOROPHENOL < 0. 010 0. 010 mg/1 JRN 03/03/2005 1636 2,4,6-TRICHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1636 2,4-DICHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1636 2,4-DIMETHYLPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1636 2,4-DINITROPHENOL < 0. 025 0.025 mg/1 JRN 03/03/2005 1636 2,4-DINITROTOLUENE < 0.010 0.010 mg/1 JRN 03/03/2005 1636 2,6-DINITROTOLUENE < 0.010 0.010 mg/1 JRN 03/03/2005 1636 2-CHLORONAPHTHALENE < 0.010 0.010 mg/1 JRN 03/03/2005 1636 2-CHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1636 2-METHYL-4,6-DINITROPHENOL < 0.025 0. 025 mg/1 JRN 03/03/2005 1636 2-METHYLNAPHTHALENE < 0.010 0. 010 mg/1 JRN 03/03/2005 1636 2-METHYLPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1636 2-NITROANILINE < 0.010 0.010 mg/1 JRN 03/03/2005 1636 2-NITROPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1636 3,3'-DICHLOROBENZIDINE < 0 010 0.010 mg/1 JRN 03/03/2005 1636 3-NITROANILINE < o. 010 0.010 mg/1 JRN 03/03/2005 1636 4-BROMOPHENYL PHENYL ETHER < 0 .010 0.010 mg/1 JRN 03/03/2005 1636 4 -CHLORO-3-METHYL.PHENOL < 0. 010 0.010 mg/1 JRN 03/03/2005 1636 4-CHLOROANILINE < 0. 010 0.010 mg/1 JRN 03/03/2005 1636 4-CHLOROPHENYL PHENYL ETHER < 0. 010 0.010 mg/1 JRN 03/03/2005 1636 4-METHYLPHENOL < 0.010 0 010 mg/1 JRN 03/03/2005 1636 4-NITROANILINE < 0 010 0. 010 mg/1 JRN 03/03/2005 1636 4-NITROPHENOL < 0 025 0 .025 mg/1 JRN 03/03/2005 1636 ACENAPHTHENE < 0 .010 0 .010 mg/1 JRN 03/03/2005 1636 ACENAPHTHYLENE < 0 .010 0. 010 mg/1 JRN 03/03/2005 1636 ANTHRACENE < 0.010 0.010 mg/1 JRN 03/03/2005 1636 BENZO(A)ANTHRACENE < 0.010 0.010 mg/1 JRN 03/03/2005 1636 BENZO(A)PYRENE < 0.010 0.010 mg/1 JRN 03/03/2005 1636 BENZO(B)FLUORANTHENE < 0.010 0.010 mg/1 JRN 03/03/2005 1636 BENZO{G,H,I)PERYLENE < 0. 010 0.010 mg/1 JRN 03/03/2005 1636 BENZO{K)FLUORANTHENE < 0.010 0.010 mg/1 JRN 03/03/2005 1636 BENZOIC ACID < 0.050 0.050 mg/1 JRN 03/03/2005 1636 BENZYL ALCOHOL < 0.010 0.010 mg/1 JRN 03/03/2005 1636 BIS(2-CHLOR6ETHOXY)METHANE < 0.010 0.010 mg/1 JRN 03/03/2005 1636 815(2-CHLOROETHYL)ETHER < 0.010 0 010 mg/1 JRN 03/03/2005 1636 815(2-CHLOROISOPROPYL)ETHER < 0.010 0.010 mg/1 JRN 03/03/2005 1636 Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I fl 16 E. Durst Avenue I Greemvoml. SC 29649 I (864) 229-4413 I Fax (864) 229-7119 I DAIIS I FLOYD LABORATORY ANALYSIS REPORT I NC Cenijication Number: 25 I Client TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD I HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Contact Pem Carter Page 34 of 88 Report ID: AC1040 Client ID: DUP-4 Sample ID L05022303-04 I Date Collected: 02/22/2005 0000 Matrix GW/Chemw Date Received 02/22/2005 Parameter Result Qual RDL units Analyst Date Time I BIS(2-ETHYLHEXYL)PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636 I BUTYL BENZYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636 CHRYSENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636 D1-N-BUTYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636 D1-N-OCTYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636 I DIBENZ(A_, HJ ANTHRACENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1636 DIBENZOFURAN ' 0.010 0.010 mg/1 JRN 03/03/2005 1636 DIETHYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636 DIMETHYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636 I FLUORANTHENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636 FLUORENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636 HEXACHLOROBENZENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636 I HEXACHLOROBUTADIENE ' 0. 010 o. 010 mg/1 JRN 03/03/2005 1636 HEXACHLOROCYCLOPENTADIENE ' 0.010 0 010 mg/1 JRN 03/03/2005 1636 HEXACHLOROETHANE ' 0. 010 0 010 mg/1 JRN 03/03/2005 1636 INDENO(l,2,3-CD)PYRENE ' 0.010 0 .010 mg/1 JRN 03/03/2005 1636 I ISOPHORONE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636 N-NITROSOOI-N-PROPYLAMINE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636 N-NITROSOOIPHENYLAMINE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1636 NAPHTHALENE ' 0.010 0 010 mg/1 JRN 03/03/2005 1636 I NITROBENZENE ' 0.010 0 010 mg/1 JRN 03/03/2005 1636 PENTACHLOROPHENOL ' 0.025 0 .025 mg/1 JRN 03/03/2005 1636 PHENANTHRENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1636 I' PHENOL ' 0.010 0. 010 mg/1 JRN 03/03/2005 1636 PYRENE ' 0.010 0 010 mg/1 JRN 03/03/2005 1636 SW846 8270C DOWTHERM 1, l' -Bl PHENYL ' 0 .010 0 .010 mg/1 JRN 03/03/2005 1636 I BIPHENYL ETHER < 0 .010 0.010 mg/1 JRN 03/03/2005 1636 Volatile Organics SW846 8260B I 1,1,1-TRICHLOROETHANE ' 0.0010 0 .0010 mg/1 PAP 02/24/2005 0951 1,1,2,2-TETRACHLOROETHANE ' 0 .0010 0. 0010 mg/1 PAP 02/24/2005 0951 1,1,2-TRICHLOROETHANE ' 0 .0010 0 .0010 mg/1 PAP 02/24/2005 0951 1,1-DICHLOROETHANE ' 0 .0010 0. 0010 mg/1 PAP 02/24/2005 0951 I 1,1-DICHLOROETHENE < 0 0010 0.0010 mg/1 PAP 02/24/2005 0951 1,2-DICHLOROETHANE ' 0.0010 0 0010 mg/1 PAP 02/24/2005 0951 1,2-DICHLOROPROPANE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0951 I 2-BUTANONE ' 0 .0050 0 . 0050 mg/1 PAP 02/24/2005 0951 2-HEXANONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0951 4-METHYL-2-PENTANONE ' 0 0050 0.0050 mg/1 PAP 02/24/2005 0951 ACETONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0951 I Davis & Floyd, Inc. I PO Drawer 428 I Crecnwoorl, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (H64) 229-4.t 13 I Fax (864) 229-7119 I I I I I I I I I I I I I I I I I I I DAYIS FLCWD Client Contact Client Matrix Parllll!eter BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROB.ENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE ID: CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-0ICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) Prep Procedure Analytical Prep Procedures1 DOWTHERM 8270 SVOC PREP LABORATORY ANALYSIS REPORT NC Certification Number: 25 TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Pem Carter Page 35 of 88 Report ID: AC1040 DUP-4 Sample ID L05022303-04 Date Collected: 02/22/2005 0000 GW/ChemW Date Received 02/22/2005 Result Qual RDL Units Analyst Date Time ' 0. 0010 0 . 0010 mg/1 PAP 02/24/2005 0951 ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0951 ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 0951 ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0951 ' 0. 0010 0 . 0010 mg/1 PAP 02/24/2005 0951 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951 0.0018 0.0010 mg/1 PAP 02/24/2005 0951 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951 0.0012 0.0010 mg/1 PAP 02/24/2005 0951 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951 0.0054 0.0010 mg/1 PAP 02/24/2005 0951 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951 ' 0.0020 0.0020 mg/1 PAP 02/24/2005 0951 Method Analyst Prep Date SW846 35008 DBC 02/28/2005 0800 SW846 3510C DBC 02/28/2005 0800 Davis 8, Floyd. Inc. I PO Drawer 42a I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood. SC 2%49 I (864) 229-441 :I I Fax (864) 229-7119 DA.YIS FL6YD LABORATORY ANALYSIS REPORT NC Certification Number: 25 Client TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Contact Pem Carter Page 36 of 88 Report ID: AC1040 Client ID: TRIP BLANK-3 Sample ID L05022303-05 Date Collected: 02/08/2005 0900 Matrix : GW/ChemW Date Received 02/22/2005 Parameter Result Qual RDL Units Analyst Date Time Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE < 0 .0010 0 .0010 mg/1 PAP 02/24/2005 0801 1,1,2,2-TETRACHLOROETHANE < o. 0010 0 .0010 mg/1 PAP 02/24/2005 0801 1,1,2-TRICHLOROETHANE < 0 .0010 o. 0010 mg/1 PAP 02/24/2005 0801 1,1-Dl~LOROETHANE < 0 .0010 o. 0010 mg/1 PAP 02/24/2005 0801 1,1-DICHLOROETHENE < o. 0010 0. 0010 mg/1 PAP 02/24/2005 0801 1,2-DICHLOROETHANE < 0. 0010 0. 0010 mg/1 PAP 02/24/2005 0801 l,2-DICHLOROPROPANE < 0. 0010 0 . 0010 mg/1 PAP 02/24/2005 0801 2-BUTANONE < 0 .0050 0.0050 mg/1 PAP 02/24/2005 0801 2-HEXANONE < 0 .0050 0.0050 mg/1 PAP 02/24/2005 0801 4-METHYL-2-PENTANONE < 0 .0050 0.0050 mg/1 PAP 02/24/2005 0901 ACETONE < 0.0050 0.0050 mg/1 PAP 02/24/2005 0801 BENZENE < 0. 0010 o. 0010 mg/1 PAP 02/24/2005 0801 BROMODICHLOROMETHANE < 0 .0010 0 .0010 mg/1 PAP 02/24/2005 0801 BROMOFORM < o. 0010 0 .0010 mg/1 PAP 02/24/2005 0801 BR OMO METHANE < 0 .0010 o. 0010 mg/1 PAP 02/24/2005 0801 CARBON DISULFIDE < 0.0010 0.0010 mg/1 PAP 02/24/2005 0801 CARBON TETRACHLORIDE < 0. 0010 0 .0010 mg/1 PAP 02/24/2005 0801 CHLOROBENZENE < 0 .0010 0 .0010 mg/1 PAP 02/24/2005 0801 CHLOROETHANE < 0 .0010 0 .0010 mg/1 PAP 02/24/2005 0801 CHLOROFORM < 0.0010 0.0010 mg/1 PAP 02/24/2005 0801 CHLOROMETHANE < 0.0010 0.0010 mg/1 PAP 02/24/2005 0801 CIS-1,2-DICHLOROETHENE < 0 .0010 0.0010 mg/1 PAP 02/24/2005 0801 CIS-1,3-DICHLOROPROPENE < 0. 0010 0.0010 mg/1 PAP 02/24/2005 0801 DIBROMOCHLOROMETHANE < 0. 0010 0.0010 mg/1 PAP 02/24/2005 0801 ETHYLBENZENE < 0 .0010 0.0010 mg/1 PAP 02/24/2005 0901 METHYLENE CHLORIDE < 0 .0010 0.0010 mg/1 PAP 02/24/2005 0801 STYRENE < 0 .0010 0.0010 mg/1 PAP 02/24/2005 0801 TETRACHLOROETHENE < 0' 0010 0.0010 mg/1 PAP 02/24/2005 0801 TOLUENE < 0 .0010 0.0010 mg/1 PAP 02/24/2005 0801 TRANS-1,2-DIOILOROETHENE < 0 .0010 0.0010 mg/1 PAP 02/24/2005 0801 TRANS-1,J-DICHLOROPROPENE < 0 .0010 0.0010 mg/1 PAP 02/24/2005 0801 TRICHLOROETHENE < 0.0010 0.0010 mg/1 PAP 02/24/2005 0801 VINYL ACETATE < 0.0010 0.0010 mg/1 PAP 02/24/2005 0801 VINYL CHLORIDE < 0.0010 0.0010 mg/1 PAP 02/24/2005 0801 XYLENE (TOTAL) < 0.0020 0.0020 mg/1 PAP 02/24/2005 0801 0;ivis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2%48 I 8 I 6 E. Durst Avenue I Greenwood, SC 2%49 I (864) 229-4413 j F.ix (H(i4) 229-7119 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAVIS FL6'YD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter Client IO: V-23 Matrix : GW/Chemw Para.meter Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICHLOROETHANE 1,1-DICHLOROETHANE 1,1-D~CHLOROETHENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 2-BUTANONE 2-HEXANONE 4-METHYL-2-PENTANONE ACETONE BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) Wet Chemistry SW846 9060 ORGANIC CARBON, TOTAL < < < < < < < < < < < < < < < < < < < < < < < < < < < < < < < Result Qual 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0050 0.0050 0.0050 0.0050 0. 021 0.0010 0.0010 0.0010 0 0010 0 0010 0.0010 0.0010 0.0010 0.0010 0 0010 0 0010 0.0010 0. 0031 0.0010 0.0010 0.0010 0.010 0.0010 0.0010 0.0010 0.0010 0.0010 0.012 10700 NC Certification Number: 25 Project Number: 61621.01 Report Date Page 37 of as April 18, 2005 Report ID: AC1040 Sample ID L05022401-0l Date Collected: 02/23/2005 0945 Date Received 02/23/2005 RDL 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0050 0.0050 0.0050 0.0050 0.0010 0.0010 0.0010 0.0010 0.0010 0 0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0. 0010 0.0010 0.0020 500 Units mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 Analyst PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP CDC Date Time 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 124.6 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 02/24/2005 1246 03/03/2005 2002 Davis & Floyd, Inc. I PO Draw~r 428 ] Greenwood, SC 2%4fl I 81 G f:. Dui·st Avenw: I Greenwood. SC 29h49 I W64) 229-4413 I Fax (8G4) 229-71 19 D~IS FLMD Client Contact Client ID: Matrix Parameter Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICHLOROETHANE 1,1-DICHLOROETHANE 1,1-DICHLOROETHENE 1,2-DICHLOROETHANE 1,2-0ICHLOROPROPANE 2-BUTANONE 2-HEXANONE 4-METHYL-2-PENTANONE ACETONE BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) Wet Chemistry SW846 9060 ORGANIC CARBON, TOTAL LABORATORY ANALYSIS REPORT NC Certification Number: 25 TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Pem Carter Page 38 of 88 Report ID: AC1040 K-28 Sample ID L05022401-02 Date Collected, 02/22/2005 1715 GW/Chemw Date Received 02/23/2005 Result Qual RDL Units Analyst Date Time ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1343 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1343 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1343 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1343 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1343 ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 1343 ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 1343 0.084 0.0050 mg/1 PAP 02/24/2005 1343 ' 0. 0050 0.0050 mg/1 PAP 02/24/2005 134 3 ' 0.0050 0 . 0050 mg/1 PAP 02/24/2005 1343 0.12 0 . 0050 mg/1 PAP 02/24/2005 1343 0.0083 0. 0010 mg/1 PAP 02/24/2005 1343 ' 0.0010 0 .0010 mg/1 PAP 02/24/2005 1343 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1343 ' 0 .0010 0. 0010 mg/1 PAP 02/24/2005 1343 ' 0 .0010 0. 0010 mg/1 PAP 02/24/2005 1343 ' 0 .0010 o. 0010 mg/1 PAP 02/24/2005 1343 ' o. 0010 0.0010 mg/1 PAP 02/24/2005 1343 ' o. 0010 0.0010 mg/1 PAP 02/24/2005 1343 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1343 ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 1343 ' o. 0010 0. 0010 mg/1 PAP 02/24/2005 1343 ' 0 .0010 0. 0010 mg/1 PAP 02/24/2005 1343 ' 0.0010 0 .0010 mg/1 PAP 02/24/2005 1343 ' 0.0010 0. 0010 mg/1 PAP 02/24/2005 1343 ' 0.0010 0. 0010 mg/1 PAP 02/24/2005 1343 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1343 ' o._0010 0.0010 mg/1 PAP 02/24/2005 1343 0.0020 0.0010 mg/1 PAP 02/24/2005 1343 ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1343 ' 0.0010 0 . 0010 mg/1 PAP 02/24/2005 1343 ' 0.0010 0 . 0010 mg/1 PAP 02/24/2005 1343 ' 0.0010 0 .0010 mg/1 PAP 02/24/2005 1343 ' 0. 0010 0 . 0010 mg/1 PAP 02/24/2005 1343 ' 0. 0020 0 . 0020 mg/1 PAP 02/24/2005 1343 60.4 12.s mg/1 CDC 03/03/2005 2027 Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2J648 I 816 E. Durst Avenue I Grecnwnod, SC 29649 I (804) 229-441 :i I Fax (864) 229-7 J 19 I I I I I I I I I I I I I I I I I I I I I LABORATORY ANALYSIS REPORT I I NC Cenijication Number: 25 Client TICONA,LLC Project Number: 61621.01 I 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Contact Pem Carter Page 39 of 88 Report ID: AC1040 I Client ID: TRIP BLANK-4 Sample ID L05022401-03 Date Collected: 02/08/2005 0900 Matrix GW/ChemW Date Received 02/23/2005 I Parameter Result Qual RDL units Analyst Date Time I Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227 1,1,2,2-TETRACHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227 I 1,1,2-TRICHLOROETHANE ' 0.0010 0. 0010 mg/1 PAP 02/24/2005 1227 1,1-DIC~LOROETHANE ' 0.0010 o. 0010 mg/1 PAP 02/24/2005 1227 1,1-DICHLOROETHENE ' 0 0010 0 .0010 mg/1 PAP 02/24/2005 1227 1,2-DICHLOROETHANE ' 0 0010 0. 0010 mg/1 PAP 02/24/2005 1227 I 1,2-DICHLOROPROPANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227 2-BUTANONE ' 0 0050 0.0050 mg/1 PAP 02/24/2005 1227 2-HEXANONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 1227 I 4-METHYL-2-PENTANONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 1227 ACETONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 1227 BENZENE ' o. 0010 0.0010 mg/! PAP 02/24/2005 1227 BROMODICHLOROMETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227 I BROMOFORM ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227 BROMOMETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227 CARBON DISULFIDE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227 CARBON TETRACHLORIDE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227 I CHLOROBENZENE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227 CHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227 CHLOROFORM ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227 I CHLO RO METHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227 CIS-1,2-DICHLOROETHENE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227 CIS-1,3-DICHLOROPROPENE ' 0.0010 0. 0010 mg/1 PAP 02/24/2005 1227 DIBROMOCHLOROMETHANE ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 1227 I ETHYLBENZENE ' 0 0010 0.0010 mg/1 PAP 02/24/2005 1227 METHYLENE CHLORIDE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 1227 STYRENE ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 1227 TETRACHLOROETHENE ' 0,0010 0. 0010 mg/1 PAP 02/24/2005 1227 I TOLUENE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 1227 TRANS-1,2-DICHLOROETHENE ' 0 0010 0.0010 mg/1 PAP 02/24/2005 1227 TRANS-1,3-DICHLOROPROPENE ' o. 0010 0.0010 mg/1 PAP 02/24/2005 1227 I TRICHLOROETHENE ' 0. 0010 0.0010 mg/! PAP 02/24/2005 1227 VINYL ACETATE ' 0 0010 0.0010 mg/1 PAP 02/24/2005 1227 VINYL CHLORIDE ' 0.0010 0 . 0010 mg/1 PAP 02/24/2005 1227 XYLENE (TOTAL} ' 0.0020 0.0020 mg/1 PAP 02/24/2005 1227 I I Dc1vis 81 Floyd, Inc. I PO DrJwer 428 I Greenwood, SC 29()4/j I 816 E. Durst Avenue I Greenwood, SC 29649 I (8(i4l 22:.J-441 J I Fax (864) 229-7119 (' I ' ,, DAYIS I FL6YD LABORATORY ANALYSIS REPORT I NC Cenification Number: 25 I Client TICONA,LLC Project Number: 61621.01 2525 BLACKSBURG ROAD I HWY 198 SHELBY, NC 28152 Report Date April 18, 2005 Contact Pem Carter Page 40 of 88 Report ID: AC1040 Client ID: PB-01 Sample ID L05022812-0l I Date Collected: 02/22/2005 1745 Matrix : GW/ChemW Date Received 02/24/2005 Parameter Result Qual RDL Units Analyst Date Time I Somivolatile Organics I SW846 8270C 1,2,4-TRICHLOROBENZENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1715 1,2-DICHLOROBENZENE ' 0 .010 0 .010 mg/1 JRN 03/03/2005 1715 1,3-DICHLOROBENZENE ' 0 .010 0 .010 mg/1 JRN 03/03/2005 1715 I 1, 4-DICH_LOROBENZENE ' 0 .010 0.010 mg/1 JRN 03/03/2005 1715 2, 4, 5-.TRICHLOROPHENOL ' 0' 010 0. 010 mg/1 JRN 03/03/2005 1715 2,4,6-TRICHLOROPHENOL ' 0 .010 0.010 mg/1 JRN 03/03/2005 1715 2,4-0ICHLOROPHENOL ' 0.010 0. 010 mg/1 JRN 03/03/2005 1715 I 2,4-0IMETHYLPHENOL ' 0.010 0.010 mg/1 JRN 03/03/2005 1715 2,4-DINITROPHENOL ' 0. 025. 0.025 mg/1 JRN 03/03/2005 1715 2,4-DINITROTOLUENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1715 2,6-DINITROTOLUENE ' 0.010 0, 010 mg/1 JRN 03/03/2005 1715 I 2-CHLORONAPHTHALENE ' 0 .010 0 .010 mg/1 JRN 03/03/2005 1715 2-CHLOROPHENOL ' 0, 010 0 .010 mg/1 JRN 03/03/2005 1715 2-METHYL-4,6-DINITROPHENOL ' o, 025 0 .025 mg/1 JRN 03/03/2005 1715 I 2-METHYLNAPHTHALENE ' 0' 010 0, 010 mg/1 JRN 03/03/2005 1715 2-METHYLPHENOL ' 0.010 0, 010 mg/1 JRN 03/03/2005 1715 2-NITROANILINE ' 0. 010 0. 010 mg/1 JRN 03/03/2005 1715 2-NITROPHENOL ' 0. 010 0. 010 mg/1 JRN 03/03/2005 1715 I 3,3'-DICHLOROBENZIDINE ' 0. 010 0.010 mg/1 JRN 03/03/2005 1715 3-NITROANILINE ' 0 .010 0. 010 mg/1 JRN 03/03/2005 1715 4-BROMOPHENYL PHENYL ETHER ' 0 .010 0.010 mg/1 JRN 03/03/2005 1715 4-CHLOR0-3-METHYLPHENOL ' 0 .010 0. 010 mg/1 JRN 03/03/2005 1715 I 4-0ILOROANILINE ' o, 010 0.010 mg/1 JRN 03/03/2005 1715 4 -CHLOROPHENYL PHENYL ETHER ' 0.010 0' 010 mg/1 JRN 03/03/2005 1715 4-METHYLPHENOL ' 0. 010 o, 010 mg/1 JRN 03/03/2005 1715 I 4-NITROANILINE ' 0 .010 0 .010 mg/1 JRN 03/03/2005 1715 4-NITROPHENOL ' 0 . 025 0' 025 mg/1 JRN 03/03/2005 1715 ACENAPHTHENE ' 0' 010 0.010 mg/1 JRN 03/03/2005 1715 ACENAPHTHYLENE ' 0 .010 0. 010 mg/1 JRN 03/03/2005 1715 I ANTHRACENE ' 0 .010 0.010 mg/1 JRN 03/03/2005 1715 BENZO(A)ANTHRACENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1715 BENZO (Al PYRENE ' 0, 010 0.010 mg/1 JRN 03/03/2005 1715 BENZO{B)FLUORANTHENE ' 0' 010 0.010 mg/1 JRN 03/03/2005 1715 I BENZO{G,H,I)PERYLENE ' 0' 010 0.010 mg/1 JRN 03/03/2005 1715 BENZO{K)FLUORANTHENE ' 0 .010 0. 010 mg/1 JRN 03/03/2005 1715 BENZOIC ACID ' 0 .050 0.050 mg/1 JRN 03/03/2005 1715 I BENZYL ALCOHOL ' 0, 010 0.010 mg/1 JRN 03/03/2005 1715 BIS{2-CHLOROETHOXY)METHANE ' 0' 010 0.010 mg/1 JRN 03/03/2005 1715 BIS{2-CHLOROETHYL)ETHER ' 0' 010 0.010 mg/1 JRN 03/03/2005 1715 BIS(2-CHLOROISOPROPYL)ETHER ' 0 .010 0. 010 mg/1 JRN 03/03/2005 1715 I Davis & Floyd, Inc. I PO Drawer 42H I Gr·ccnw()od, SC 2%48 I 816 E, Durst Avenue I Grecnwond, SC 2%49 I (864) 2'.!.'.)-4413 I Fax (/\(A) 229-71 1 ~l I I I I I I I I I I I I I I I I I I I DAVIS FL6YD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter Client ID: FB-01 Matrix Parameter BIS(2-ETHYLHEXYL)PHTHALATE BUTYL BENZYL PHTHALATE CHRYSENE DI-N-BUTYL PHTHALATE DI-N-OCTYL PHTHALATE DIBENZ (A., H) ANTHRACENE DIBENZOFURAN DIETHYL PHTHALATE DIMETHYL PHTHALA.TE FLUORANTHENE FLUORENE HEXACHLOROBENZENE HEXACHLOROBUTADIENE HEXACHLOROCYCLOPENTADIENE HEXACHLOROETHANE INDENO(l,2,3-CD)PYRENE ISOPHORONE N-NITROSODI-N-PROPYLAMINE N-NITROSODIPHENYLAMINE NAPHTHALENE NI TROBENZENE PENTACHLOROPHENOL PHENANTHRENE PHENOL PYRENE SW846 8270C DOWTHERM 1,1'-BIPHENYL BIPHENYL ETHER Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICHLOROETHANE l,1-0ICHLOROETHANE l,l-DICHLOROETHENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 2-BUTANONE 2-HEXANONE 4-METHYL-2-PENTANONE ACETONE GW/ChemW Result Qual 0. 010 0. 010 0. 010 0.010 0.010 0.010 0.010 0. 010 0.010 0. 010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0. 010 0.025 0.010 0.010 0.010 0.010 0 010 1.0 1.0 1.0 1.0 1.0 1. 0 1.0 s.o 5.0 5.0 16.2 NC Cenijication Number: 25 Project Number: 61621.01 Report Date Page 41 of 88 April 18, 2005 Report ID: AC1040 Sample ID L05022812-01 Date Collected: 02/22/2005 1745 Date Received RDL 0.010 0 010 0 010 0.010 0.010 0.010 0.010 0.010 0.010 0. 010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0. 010 0.010 0.010 0. 010 0.025 0.010 0.010 0.010 0.010 0.010 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 s.o s.o 5.0 units mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 rng/1 rng/1 mg/1 rng/1 mg/1 rng/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 02/24/2005 Analyst JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN JRN PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP Date Tima 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1715 03/03/2005 1216 03/03/2005 1216 03/03/2005 1216 03/03/2005 1216 03/03/2005 1216 03/03/2005 1216 03/03/2005 1216 03/03/2005 1216 03/03/2005 1216 03/03/2005 1216 03/03/2005 1216 Davis & Floyd, Inc. I PO Dr;n.ver· 428 j Greenwood, SC 2%48 I H ! 6 L Durst 1\venuc I Creenwond, SC 2964'.) I (HF,4) 129-44 ! :1 I Fax (8G4) 229-711 ~J DAJIS FLOYD Client Contact Client Matrix Parameter BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON T/:=TRACHLORIDE CHLOR08ENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE ID: CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE ETHYLBENZENE METHYLENE CHLORIDE STYRENE TETRACHLOROETHENE TETRAHYDROFURAN TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE VINYL ACETATE VINYL CHLORIDE XYLENE (TOTAL) Prep Procedure Analytical Prep Procedures, DOWTHERM 8270 SVOC PREP LABORATORY ANALYSIS REPORT TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter P'B-01 GW/ChemW < < < < < ' < < < < < < < < < < < < < < ' < < < < Method SW846 35008 SW846 3510C Result Qual 1.0 .0 .0 1 .o 1.0 1.0 1.0 .o 1 .o 1 .o 1 .o .0 1 .o 1 .0 1 .0 1.0 1.0 5. 0 1 .o 1 .o 1 .o 1. 0 1.0 1.0 2.0 Analyst DBC DBC NC Certification Number: 25 Project Number: 61621.01 Report Date April 18, 2005 Page 42 of 88 Report ID: AC1040 Sample ID L05022812~01 Date Collected: 02/22/2005 1745 Date Received 02/24/2005 RDL Units Analyst Date Time 1 .o ug/1 PAP 03/03/2005 1216 1 .o ug/1 PAP 03/03/2005 1216 1 .o ug/1 PAP 03/03/2005 1216 1.0 ug/1 PAP 03/03/2005 1216 .0 ug/1 PAP 03/03/2005 1216 1 .o ug/1 PAP 03/03/2005 1216 1 .0 ug/1 PAP 03/03/2005 1216 1. 0 ug/1 PAP 03/03/2005 1216 1.0 ug/1 PAP 03/03/2005 1216 1.0 ug/1 PAP 03/03/2005 1216 1.0 ug/1 PAP 03/03/2005 1216 1.0 ug/1 PAP 03/03/2005 1216 1.0 ug/1 PAP 03/03/2005 1216 1.0 ug/1 PAP 03/03/2005 1216 1 .o ug/1 PAP 03/03/2005 1216 1 .0 ug/1 PAP 03/03/2005 1216 1 .0 ug/1 PAP 03/03/2005 1216 5.0 ug/1 PAP 03/03/2005 1216 1.0 ug/1 PAP 03/03/2005 1216 1.0 ug/1 PAP 03/03/2005 1216 1.0 ug/1 PAP 03/03/2005 1216 1 .0 ug/1 PAP 03/03/2005 1216 1 .0 ug/1 PAP 03/03/2005 1216 1.0 ug/1 PAP 03/03/2005 1216 2.0 ug/1 PAP 03/03/2005 1216 Prep Date 02/28/2005 0800 02/28/2005 0800 Davis &-Floyd, Inc. I PO Drawe1· 428 I Creenwoorl, SC 29(i413 I BI h E. Durst Avenue I CrC'enwornl, SC 2%4') I (864) 229-44 lJ I Fax ((H)4) 22:J-7 I 19 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAVIS FLijYD Client Contact LABORATORY ANALYSIS REPORT TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Cenijication Number: 25 Project Number: 61621.01 Report Date April 18, 2005 Page 43 of 88 Report ID: AC1040 QC Summary Data Davis & floyU, Inc. I PO Drawer 4'..:H I Greenwood, SC 29648 I BI fi E. Durst Avenue I Greenwood, SC '..:'."Jh4<) I (1.l(i4J :!.2':l-4413 I Fax (864) 229-711 lJ D\VIS FLOYD LABORATORY ANALYSIS REPORT Sample ID L05022007-01 L05022007-02 L05022007-03 L05022007-04 Client Contact TICONA, LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem carter NC Cenijication Number: 25 Project Number: 61621.01 Report Date Page 44 of 88 April 18, 2005 Report ID: AC1040 QC Batch Report -Batch Sample List WorkGroup WG40376 Matrix GW/ChemW D~scription: vo/8260/TCL Prep Method Analtyical Method: SW846 82608 PREP ANALYTICAL Client ID •=• Date Time Date Time Analyst P-58 02/21/2005 1544 PAP F-55 02/21/2005 1620 PAP CC-33 02/21/2005 1602 PAP TRIP BLANK-2 1 02/21/2005 1204 PAP Dilution 3 1 D;wis & Floyd, Inc. I PO Drawe,· 4:W I GrL•e11wood, SC 1%48 I Ii 16 E. Durst Avenue I Creenwoud, SC 2%-f9 I (H64) 229-441 J I Fax (WA) 229-71 19 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAYIS FLfiYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Certification Number: 25 Project Number: 61621.01 Report Date Page 45 of 88 April 18, 2005 Report ID: AC1040 QC Batch Report -Surrogates % Recovery WorkGroup: WG40376 Matrix GW/ChemW Prep Method Analtyical Method: $W846 8260B L05022007-01 02/21/2005 1544 117 105 98 LOS022007-02 02/21/2005 1620 113 107 96 L05022007-03 02/21/2005 1602 122 105 98 L05022007-04 02/21/2005 12 04 101 103 100 DCE 1,2-DICHLOROETHANE-D4 BFB BROMOFLUOROBENZENE TOL TOLUENE-DB Davis 8, Floyd, Inc. I PO Drawer 42H I Creenwood, SC 2%48 I l.l I (j t. Dur~I Avenue I Greenwood, SC L:l(i4~) I (864) 229-44 fJ I Fax (1364) 229-711 '.l D~fIS FLOYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Cenification Number: 25 Project Number: 61621.01 Report Date April 18, 2005 Page 46 of 88 Report ID: AC1040 QC Batch Report -Batch Sample List WorkGroup WG40399 Matrix GW/Chemw D~scription: VO/8260/TCL RDL OF' 1 Prep Method Analtyical Method: SW846 82608 ANALYTICAL Sample ID Client ID Rud PRP!P Date Time Date Time Analyst Dilution 105021805-01 HH-77 L05021805-02 HH-48 105021805-03 C-49 105021805-04 FF-34 L05021805-05 FF-62 L05021805-06 GG-61 105021805-07 T-35 105021805-08 AA-54 L05021805-09 EE-58 MB40399:l Method Blank LCS40399:l Laboratory Control Spike MS05021805-03 :40399 Matrix Spike MSD05021805-03:40399 Matrix Spike Duplicate 1 02/22/2005 1 02/22/2005 1 02/22/2005 1 02/22/2005 02/22/2005 1 02/22/2005 02/22/2005 1 02/22/2005 1 02/22/2005 02/22/2005 02/22/2005 02/22/2005 02/22/2005 1556 1328 1346 1405 1424 1442 1501 1519 1538 1033 1729 1634 1652 PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP PAP 1 1 1 1 1 D,1vis &-Floyd, Inc. I PO Drnwer 4213 I Greenwood, SC 2%48 I 81 h E. Durst Aventie I Greenwood, SC 29fi49 I /864\ n9-44 1 J I F::ix (llli4) 22Y-7 I I~ I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAVIS FL61'D LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Fem Carter NC Certification Number: 25 Project Number: 61621.01 Report Date April 18, 2005 Page 47 of BB Report ID: AC1040 QC Batch Report -Surrogates % Recovery WorkGroup: WG40399 Matrix GW/ChemW Prep Method Analtyical Method: SWB46 82608 L05021805-01 02/22/2005 1556 105 99 96 L05021805-02 02/22/2005 1328 95 97 97 L05021805-03 02/22/2005 1346 96 98 97 L05021805-04 02/22/2005 1405 99 100 98 L05021805-05 02/22/2005 1424 98 99 98 L05021805-06 02/22/2005 1442 97 99 97 L05021805-07 02/22/2005 1501 101 101 98 L05021805-08 02/22/2005 1519 100 99 98 L05021805-09 02/22/2005 1538 99 99 98 MB40399:l 02/22/2005 1033 97 98 99 LCS40399:1 02/22/2005 1729 118 104 95 MS05021805-03:40399 02/22/2005 1634 114 101 96 MSD05021805-03:40399 02/22/2005 1652 115 100 96 DCE 1,2-DICHLOROETHANE-D4 BFB BROMOFLUOROBENZENE TOL TOLUENE-DB O;wis & Floyd, Inc. I PO Druwer 428 I Greenwood, SC 29648 I Bl 6 E. Durst /\venue I Greenwood, SC 2%-+9 I (864) 229-4413 I Fax (864) 229-7119 DAYIS Filrvo LABORATORY ANALYSIS REPORT Client Contact TICONA, LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem carter QC Batch Report-Method Blanks WorkGroup: WG40399 B~ank MB40399:1 Para.motor Result Qual Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE < 0.0010 1 , 1, 2 , 2 -_TETRACHLOROETHANE < 0.0010 l,l,2~TRIC1-iLOROETHANE < 0. 0010 1,1-DICHLOROETHANE < 0.0010 1,1-DICHLOROETHENE < 0.0010 1,2-DICHLOROETHANE < 0.0010 1,2-DICHLOROPROPANE < 0.0010 2-BUTANONE < 0.0050 2-HEXANONE < 0.0050 4-METHYL-2-PENTANONE < 0. 0050 ACETONE < 0 0050 BENZENE < 0 0010 BROMODICHLOROMETHANE < 0. 0010 BROMOFORM < 0.0010 BROMOMETHANE < 0 0010 CARBON DISULFIDE < 0 0010 CARBON TETRACHLORIDE < 0 .0010 CHLOROBENZENE < 0 .0010 CHLOROETHANE < 0 0010 CHLOROFORM < o. 0010 CHLOROMETHANE < 0.0010 CIS-1,2-DICHLOROETHENE < 0.0010 CIS-1,3-DICHLOROPROPENE < 0.0010 DIBROMOCHLOROMETHANE < 0.0010 ETHYLBENZENE < 0.0010 METHYLENE CHLORIDE < 0 0010 STYRENE < 0.0010 TETRACHLOROETHENE < 0.0010 TOLUENE < 0.0010 TRANS-1,2-DICHLOROETHENE < 0.0010 TRANS-1,3-DICHLOROPROPENE < 0.0010 TRICHLOROETHENE < 0.0010 VINYL ACETATE < 0.0010 VINYL CHLORIDE < 0.0010 XYLENE (TOTAL) < 0.0020 NC Cenijication Number: 25 Project Number: 61621.01 Report Date Page 48 of 88 Matrix: GW/Chemw RDL Units 0 . 0010 mg/1 0. 0010 mg/1 0. 0010 mg/1 0 .0010 mg/1 0. 0010 mg/1 0 0010 mg/1 0.0010 mg/1 0.0050 mg/1 0.0050 mg/1 0.0050 mg/1 0.0050 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/! 0.0010 mg/1 0.0010 mg/1 0.0010 mg/! 0 0010 mg/1 0 .0010 mg/1 0. 0010 mg/1 0 0010 mg/1 0.0010 rng/1 0.0010 rng/1 0.0010 mg/1 0.0010 mg/1 0.0010 rng/1 0.0010 rng/1 0.0010 rng/1 0.0010 rng/1 0.0010 rng/1 0.0010 rng/1 0.0010 mg/! 0.0010 rng/1 0.0020 rng/1 April 18, 2005 Report ID: AC1040 Analyst Date PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02 /22 /2 005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02 /22 /2 005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 PAP 02/22/2005 Time 1033 1033 1033 1033 1033 1033 1033 1033 1033 1033 1033 1033 1033 1033 1033 1033 1033 1033 1033 1033 1033 1033 1033 1033 1033 1033 103 3 1033 1033 1033 1033 1033 1033 1033 1033 D.ivis &· Floyd, Inc. I PO Drawer 42R I Greenwood, SC 29648 I 81 h E. Durst Avenue I Greenwood, SC 29649 I (86·1) 229-4413 I Fax (864) 229-7 ! 1 Y I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAVIS FL6YD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Cenijication Number: 25 Project Number, 61621.01 Report Date Page 49 of as April 18, 2005 Report ID: AC1040 QC Batch Report -Matrix Spikes and Duplicates WorkGroup: WG40399 MS/MSD MS0S0:21805-03: 40399 MSD05021805-03:40399 1,1,1-TRICHLOROETHANE 0.0500 1,1,2-TRICHLOROETHANE 0.0500 1, 1-DICH_LOROETHENE 0.0500 1,2-DioiLOROETHANE 0.0500 1,2-DICHLOROPROPANE 0.0500 2-BUTANONE 0.0500 BENZENE 0.0500 CARBON TETRACHLORIDE 0.0500 CHLOROBENZENE 0.0500 CHLOROFORM 0.0500 DIBROMOCHLOROMETHANE 0.0500 TETRACHLOROETHENE 0.0500 TOLUENE 0.0500 TRICHLOROETHENE 0.0500 VINYL CHLORIDE 0.0500 1,1,1-TRICHLOROETHANE 0.0500 1,1,2-TRICHLOROETHANE 0.0500 1,1-DICHLOROETHENE 0.0500 1,2-DICHLOROETHANE 0.0500 1,2-DICHLOROPROPANE 0.0500 2-BUTANONE 0.0500 BENZENE 0.0500 CARBON TETRACHLORIDE 0.0500 CHLOROBENZENE 0.0500 CHLOROFORM 0.0500 DIBROMOCHLOROMETHANE 0.0500 TETRACHLOROETHENE 0.0500 TOLUENE 0.0500 TRICHLOROETHENE 0.0500 VINYL CHLORIDE 0.0500 NOTB1 MS/MSD \ recoveries are not evaluated if the Matrix GW/Chemw Prep Method Analtyical Method: SWB46 8260B < 0.00100 0.0517 mg/1 103 88-124 < 0.00100 0. 0-481 mg/1 96 88-128 < 0.00100 0.0566 mg/1 ll3 71-130 < o. 00100 0.0541 mg/1 108 78-143 < 0 .00100 0. 0455 mg/1 91 91-118 < 0. 00500 0. 0477 mg/1 95 28-199 < o. 00100 0.0514 mg/1 103 77-123 < 0. 00100 0.0557 mg/1 lll 63-135 < 0.00100 0. 04 98 mg/1 100 78-123 < 0.00100 0.0558 mg/1 ll2 75-135 < 0.00100 0.0526 mg/1 105 88-133 < 0.00100 0.0508 mg/1 102 69-123 < 0.00100 0. 04 96 mg/1 99 85-117 < 0.00100 0.0499 mg/1 100 75-121 < 0.00100 0. 0453 mg/1 91 47-136 0.0550 mg/1 llO 6 15 88-124 0. 04 94 mg/1 99 3 17 88-128 0.0584 mg/1 ll7 3 17 71-130 0.0552 mg/1 110 2 20 78-143 0.0456 mg/1 91 0 14 91-118 0.0468 mg/1 94 2 31 28-199 0.0509 mg/1 102 17 77-123 0.0576 mg/1 ll5 3 20 63-135 0.0512 mg/1 102 3 17 78-123 0.0580 mg/1 ll6 4 17 75-135 0.0543 mg/1 109 15 88-133 0.0523 mg/1 105 3 17 69-123 0.0509 mg/1 102 3 15 85-117 0.0513 mg/1 103 3 17 75-121 0. 04 64 mg/1 93 2 19 47-136 sample concentration is greater than four times the spike added. Dcivis & Floyd, Inc. I PO Drawer 42R I Greenwood, SC 29648 I S-1 (1 F.. Durst Avenue I Creenwoud, SC 2%4~ I (864) 22~)-441 J I Fax (864) 229-7119 D~lS FLtJYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Certification Number: 25 Project Number: 61621.01 Report Date Page SO of 88 April 18, · 2005 Report ID: AC1040 QC Batch Report -Laboratory Control Standards and Duplicates WorkGroup: WG40399 Matrix GW/ChemW L~S LCS40399:l Prep Method Analtyical Method: SW846 8260B 1,1,1-TRICHLOROETHANE 0.0200 0.0228 mg/1 114 79-127 1,1,2-TRICHLOROETHANE 0.0200 0 0208 mg/1 104 B3-143 1,1-DICHLOROETHENE 0 0200 0.0244 mg/1 122 63-141 1,2-DICHLOROETHANE o. 0200 0. 024 0 mg/1 120 79-147 1,2-DICHLOROPROPANE 0 . 0200 0.0187 mg/1 93 86-130 2-BUTANONE 0 0200 0 .0215 mg/1 107 52-190 BENZENE 0 .0200 0. 0217 mg/1 109 78-123 CARBON TETRACHLORIDE 0. 0200 0.0235 mg/1 117 58-132 CHLOROBENZENE 0 0200 0.0212 mg/1 106 81-124 CHLOROFORM 0 . 0200 0 . 0244 mg/1 122 75-138 DIBROMOCHLOROMETHANE 0.0200 0 0215 mg/1 107 82-137 TETRACHLOROETHENE 0.0200 0 .0210 mg/1 105 71-120 TOLUENE o. 0200 0. 0211 mg/1 106 81-121 TRICHLOROETHENE 0.0200 0 0222 mg/1 111 ?6-120 VINYL CHLORIDE o. 0200 0 0180 mg/1 90 51-138 Davis & Floyd, Inc. I PO Drawer 428 ) Greenwood, SC 19648 I 816 E. Durst Avenue I Greenwood, SC 2%49 I (8641 2'.:9-4413 I Fax W64) 229-7119 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I Di\:VIS FLOYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Cenification Number: 25 Project Number: 61621.01 Report Date Page 51 of as April 18, 2005 Report ID: AC1040 QC Batch Report -Batch Sample List WorkGroup WG40428 Matrix GW/ChemW □e._scription: V0/8260/TCL RDL of 1 Prep Method Analtyical Method: SW846 8260B PREP ANALYTICAL Sample ID Client ID Run# Date Time Date Time Analyst L05021803-01 DUP-1 1 02/24/2005 0837 PAP LOS021803-06 EB-01 02/24/2005 0819 PAP L05021,8.'05-10 TRIP BLANK 02/24/2005 0743 PAP L05022303-01 PEW-1 02/24/2005 0856 PAP L05022303-02 PEW-3 1 02/24/2005 0915 PAP L05022303-03 PEW-4 1 02/24/2005 0933 PAP L050223 03-04 DUP-4 1 02/24/2005 0951 PAP L05022303-05 TRIP BLANK-3 02/24/2005 0801 PAP L0502240l~Ol V-23 02/24/2005 1246 PAP L05022401-02 K-28 1 02/24/2005 1343 PAP L05022401-03 TRIP BLANK-4 1 02/24/2005 1227 PAP MB40428:l Method Blank 1 02/24/2005 0722 PAP LCS40428:1 Laboratory Control Spike 1 02/24/2005 1105 PAP MS05022303-02:40428 Matrix Spike 1 02/24/2005 1028 PAP M8D05022303-02:40428 Matrix Spike Duplicate 02/24/2005 1047 PAP Dilution 1 1 1 1 1 1 1 1 1 Davis & Floyrl, Inc. I PO Drawer 42H I Greenwood, SC 29648 I fil h E. Ours! Avenue I Creenwonr!, SC 19649 I (864) 129-4413 I Fax (864) 229-7119 LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Cenijication Number: 25 Project Number: 61621.01 Report Date April 18, 2005 Page 52 of 88 Report ID: AC1040 QC Batch Report -Surrogates % Recovery WorkGroup: WG40428 Matrix GW/ChemW Prep Method Analtyical Method: SW846 82608 L05021803-01 02/24/2005 0837 110 102 97 LOS021803-06 02/24/2005 0819 107 103 98 LOS021805-10 02/24/2005 0743 102 103 97 L05022303-01 02/24/2005 0856 109 104 95 LOS022303-02 02/24/2005 0915 111 104 96 L05022J03-03 02/24/2005 0933 109 104 97 L05022303-04 02/24/2005 0951 109 104 96 L05022303-0S 02/24/2005 0801 102 100 95 L05022401-0l 02/24/2005 1246 103 105 95 105022401-02 02/24/2005 1343 93 101 96 L05022401-03 02/24/2005 1227 116 107 97 MB40428:l 02/24/2005 0722 101 101 97 LCS40428:l 02/24/2005 1105 115 106 96 MS05022303-02:40428 02/24/2005 1028 114 106 95 MSD05022303-02:4042B 02/24/2005 1047 114 105 96 DCE 1,2-DICHLOROETHANE-D4 BFB BROMOFLUOROBENZENE TOL TOLUENE-DB Davis & Floyd, Inc. I PO Drawer 428 / Greenwood, SC 29648 I 816 F.. Durst Avenue I Greenwood, SC 2%49 I (864) 229-441 J I Fax {B64) 229-7119 I I! I I 11 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAYIS FLMD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter QC Batch Report -Method Blanks WorkGroup, WG40t28 Bl,ank MB40428:1 Parameter Result Qual Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE ' 0 0010 1,1,2,2-TETRACHLOROETHANE ' 0 0010 1, 1, 2-.TRICHLOROETHANE ' 0 .0010 1,1-DICHLOROETHANE ' 0 .0010 1,1-DICHLOROETHENE ' 0. 0010 1,2-DICHLOROETHANE ' . 0 0010 1,2-DICHLOROPROPANE ' 0 0010 2-BUTANONE ' 0.0050 2-HEXANONE ' 0.0050 4-METHYL-2-PENTANONE ' 0.0050 ACETONE ' 0.0050 BENZENE ' 0.0010 BROMODICHLOROMETHANE ' 0.0010 BROMOFORM ' 0.0010 BROMOMETHANE ' 0.0010 CARBON DISULFIDE ' 0.0010 CARBON TETRACHLORIDE ' 0.0010 CHLOROBENZENE ' 0.0010 CHLOROETHANE ' 0.0010 CHLOROFORM ' 0.0010 CHLOROMETHANE ' 0 0010 CIS-1,2-DICHLOROETHENE ' o. 0010 CIS-1,3-DICHLOROPROPENE ' 0 .0010 DIBROMOCHLOROMETHANE ' 0. 0010 ETHYLBENZENE ' 0 0010 METHYLENE CHLORIDE ' 0.0010 STYRENE ' 0.0010 TETRACHLOROETHENE ' 0.0010 TOLUENE ' 0 .0010 TRANS-1,2-DICHLOROETHENE ' 0.0010 TRANS-1,3-DICHLOROPROPENE ' 0.0010 TRICHLOROETHENE ' 0.0010 VINYL ACETATE ' 0.0010 VINYL CHLORIDE ' 0.0010 XYLENE (TOTAL) ' 0.0020 NC Cenijication Number: 25 Project Number: 61621.01 Report Date April 18, 2005 Page 53 of 88 Report ID: AC1040 Matrix: GW/Chemw RDL units Analyst Date Time 0.0010 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0.0050 mg/1 PAP 02/24/2005 0722 0.0050 mg/1 PAP 02/24/2005 0722 0.0050 mg/1 PAP 02/24/2005 0722 0.0050 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0 0010 mg/1 PAP 02/24/2005 0722 0 0010 mg/1 PAP 02/24/2005 0722 0 .0010 mg/1 PAP 02/24/2005 0722 0. 0010 mg/1 PAP 02/24/2005 0722 0. 0010 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0. 0010 mg/1 PAP 02/24/2005 0722 0 .0010 mg/1 PAP 02/24/2005 0722 0. 0010 mg/1 PAP 02/24/2005 0722 0. 0010 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0.0010 mg/1 PAP 02/24/2005 0722 0 0010 mg/1 PAP 02/24/2005 0722 0.0020 mg/1 PAP 02/24/2005 0722 I D,wis ,I(.: Floyd, Inc. I PO Drawer 42/-1 I Greenwurnl, SC 291)4/l I 816 E. Durst Ave1111e I Greenwood, SC 29(i49 I (B64) 221)-4413 I Fax (8fi4) 229-7"119 D:\YIS FLOYD LABORATORY ANALYSIS REPORT Client Contact TICONA, LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Cenification Number: 25 Project Number: 61621.01 Report Date Page 54 of 88 April 18, 2005 Report ID: AC1040 QC Batch Report -Matrix Spikes and Duplicates WorkGroup: WG40428 MS05022303-02:40428 MSD05022303-.02: 40428 1,1,1-TRICHLOROETHANE 0 .osoo 1,1,2-TRICHLOROETHANE 0 . 0500 1,1-DICHLOROETHENE 0.0500 1,2-DitjH . .OROETHANE 0.0500 1,2-DICHLOROPROPANE 0.0500 2.-BUTANONE 0.0500 BENZENE 0 .0500 CARBON TETRACHLORIDE 0. 0500 CHLOROBENZENE 0.0500 CHLOROFORM 0.0500 DIBROMOCHLOROMETHANE 0 -0500 TETRACHLOROETHENE o. 0500 TOLUENE 0. 0500 TRICHLOROETHENE 0.0500 VINYL CHLORIDE 0.0500 1,1,1-TRICHLOROETHANE 0. 0500 1,1,2-TRICHLOROETHANE 0 .0500 1,1-DICHLOROETHENE 0. 0500 1,2-DICHLOROETHANE 0.0500 1,2-DICHLOROPROPANE 0.0500 2-BUTANONE 0.0500 BENZENE 0 .0500 CARBON TETRACHLORIDE 0. 0500 CHLOROBENZENE 0 .0500 CHLOROFORM 0. 0500 DIBROMOCHLOROMETHANE 0 .0500 TETRACHLOROETHENE 0.0500 TOLUENE 0 .0500 TRICHLOROETHENE o. 0500 VINYL CHLORIDE 0 . 0500 NOTB: MS/MSD \ recoveries are not evaluated if the Matrix GW/Chemw Prep Method Analtyical Method: SW846 82608 < 0.00100 0 .0555 mg/1 111 88-124 < 0.00100 0 .0474 mg/1 95 88-128 '0. 00100 0 . 0538 mg/1 108 71-130 ' 0 . 00100 0 . 0565 mg/1 113 78-143 ' 0 . 00100 o . 0463 mg/1 93 91-118 ' 0 .00500 0.0444 mg/1 89 28-199 ' 0 .00100 0.0507 mg/1 101 77-123 <.0 .00100 0.0574 mg/1 115 63-135 < 0.00100 0.0514 mg/1 103 78-123 < 0.00100 0.0564 mg/1 113 75-135 < 0.00100 0.0557 mg/1 111 88-133 ' 0.00100 0.0516 mg/1 103 69-123 < 0.00100 0.0501 mg/1 100 85-117 ' 0 .00100 0.0509 mg/1 102 75-121 ' 0 .00100 0.0400 mg/1 BO 47-136 0.0547 mg/1 109 1 15 88-124 0. 04 92 mg/1 98 ' 17 88-128 o. 0511 mg/1 102 5 17 71-130 0 .0560 mg/1 112 1 20 78-143 0 .0460 mg/1 92 1 14 91-118 0.0427 mg/1 85 ' 31 28-199 0.0510 mg/1 102 17 77-123 0.0579 mg/1 116 1 20 63-135 0.0506 mg/1 101 l 17 78-123 0.0557 mg/1 111 1 17 75-135 0 . 0561 mg/1 112 15 88-133 0 .0513 mg/1 103 0 17 69-123 0. 0504 mg/1 101 15 85-117 0 . 0517 mg/1 103 2 17 75-121 0.0404 mg/1 81 1 19 47-136 sample concentration is greater than four times the spike added. Davis & Floyd, Inc. I PO Dr:1wer 428 I Creenwuud, SC 29(i48 I 81 (1 E. Durst Avcmue I Cret:nwood, SC 29649 I (/l64) 22~-441 J I fax (H64) 220-7119 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I D~IS FLMD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Cenijication Number: 25 Project Number: 61621.01 Report Date Page 55 of 88 April 18, 2005 Report ID: AC1040 QC Batch Report -Laboratory Control Standards and Duplicates WorkGroup: WG40428 Matrix· GW/ChemW LCS LCS40428:l Prep Method Analtyical Method: SW846 82608 1,1,1-TRICHLOROETHANE 0.0200 0.0231 mg/1 116 79-127 1,1,2-TRICHLOROETHANE 0.0200 0.0217 mg/1 108 B3-143 1,1-DICHLOROETHENE 0.0200 0.0220 mg/1 110 63-141 1, 2-DI,CHI..OROETHANE 0.0200 0.0250 mg/1 125 79-147 1,2-DICHLOROPROPANE 0.0200 0.0189 mg/1 95 86-130 2-BUTANONE 0.0200 0.0198 mg/1 99 52-190 BENZENE 0.0200 0. 0216 mg/1 108 7B-123 CARBON TETRACHLORIDE 0.0200 0.0248 mg/1 124 58-132 CHLOROBENZENE 0 .0200 0 0218 mg/1 109 81-124 CHLOROFORM 0.0200 0. 0242 mg/1 121 75-138 DIBROMOCHLOROMETHANE 0. 02 00 0 0240 mg/1 120 82-13 7 TETRACHLOROETHENE 0.0200 0. 0220 mg/1 110 71-120 TOLUENE 0 . 0200 0 0217 mg/1 109 81-121 TRICHLOROETHENE o. 0200 0.0215 mg/1 108 76-120 VINYL CHLORIDE o. 0200 0. 01 72 mg/1 86 51-138 Davis & rloyd, Inc. I PO Drawer 428 I Creenwood, SC 296..J.a I 8 ! h E. Dur~! Avenue I Greenwouc!, SC 29649 I (H64) 229-44 1 J I F,1x (864) 229-71 ! 9 Sample ID L05022812-01 L05022812-0l MB4048,7·: 1 LCS40487: 1 MS05022810-04 LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Cenification Number: 25 Project Number: 61621.01 Report Date Page 56 of 88 April 18, 2005 Report ID: AC1040 QC Batch Report -Batch Sample List WorkGroup WG40487 Matrix GW/ChemW D~scription: vo/8260/TCL Prep Method Analtyical Method: SW846 8260B PREP ANALYTICAL Client IC Run# Date Time Date Time Analyst FB-01 1 03/03/2005 1216 PAP FB-01 2 03/03/2005 1216 PAP Method Blank 1 03/03/2005 1119 PAP Laboratory Control Spike 03/03/2005 1748 PAP :40487 Matrix Spike 1 03/03/2005 1331 PAP Dilution 1 1 MSD05022810-04:40487 Matrix Spike Duplicate 1 03/03/2005 1349 PAP Davis & F!oyd, Inc. I PO Drawer 42H I Greenwood, SC 2%48 I 816 E. Durst Avenue I Creenwood, SC 29649 I {1364) 12~-44 ! 3 I fax (H64) 229-7119 I I I I I I I I I I I I I I! I I I I I I I I I I I I I I I I I I I I I I DAYIS FLMD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Certification Number: 25 Project Number: 61621.01 Report Date April 18, 2005 Page 57 of 88 Report ID: AC1040 QC Batch Report -Surrogates % Recovery WorkGroup: WG40487 Matrix GW/Chemw Prep Method Analtyical Method: SW846 82608 LOS022812-0l 03/03/2005 1216 93 96 98 L0502281~-01 03/03/2005 1216 93 M8404S7,! i 03/03/2005 1119 95 96 98 LCS40487:l 03/03/2005 l "48 108 96 97 MS05022810-04:40487 03/03/2005 1331 112 100 97 MSD05022810-04:40487 03/03/2005 1349 116 100 98 DCE l,2-DICHLOROETHANE-04 BFB BROMOFLUOROBENZENE TOL TOLUENE-DB I Davis 8, Floyd, Inc. / PO Drawer 428 I Greenwood, SC 29648 I 81 fi I::. Durst Avenue I Greenwood, SC 29fi49 I {864} 229-4413 I Fax (864) 229-7119 Dl\VIS FLOYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter QC Batch Report -Method Blanks WorkGroup: WG40487 Bl~nk MB40487: l Paramoter Result Qual Volatile Organics SW846 8260B 1,1,1-TRICHLOROETHANE ' 1.0 1,1,2,2-TETRACHLOROETHANE ' 1.0 1,1,2-TRICHLOROETHANE ' 1.0 1,1-DICHLOROETHANE ' 1. 0 1,1-DICHLOROETHENE ' 1 .o 1,2-DICHLOROETHANE ' 1 0 1,2-DICHLOROPROPANE ' 1.0 2-BUTANONE ' 5 .o 2-HEXANONE ' 5.0 4-METHYL-2-PENTANONE ' 5.0 ACETONE ' 5.0 BENZENE ' 1.0 BROMODICHLOROMETHAN'E ' 1 .o BROMOFORM ' 1.0 BROMOMETHAN'E ' 1.0 CARBON DISULFIDE ' 1.0 CARBON TETRACHLORIDE ' .o CHLOROBENZENE ' 1.0 CHLO RO ETHANE ' 1.0 CHLOROFORM ' 1.0 CHLOROMETHANE ' 1.0 CIS-1,2-DICHLOROETHENE ' 1.0 CIS-1,3-DICHLOROPROPENE ' .0 DIBROMOCHLOROMETHANE ' 1 .o ETHYLBENZENE ' 1 .o METHYLENE CHLORIDE ' 1.0 STYRENE ' 1.0 TETRACHLOROETHENE ' 1.0 TOLUENE ' 1.0 TRANS-1,2-DICHLOROETHENE ' 1.0 TRANS-1,3-DICHLOROPROPENE ' 1.0 TRICHLOROETHENE ' 1 0 VINYL ACETATE ' 1.0 VINYL CHLORIDE ' .0 XYLENE (TOTAL) ' ' .0 NC Certification Number: 25 Project Number: 61621.01 Report Date April 18, 2005 Page 58 of 88 Report ID, AC1040 Matrix: GW/Chemw RDL Units Analyst Date Tima 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 5.0 ug/1 PAP 03/03/2005 1119 5.0 ug/1 PAP 03/03/2005 1119 5.0 ug/1 PAP 03/03/2005 1119 5.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 . 0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 1. 0 ug/1 PAP 03/03/2005 1119 . 0 ug/1 PAP 03/03/2005 1119 1 0 ug/1 PAP 03/03/2005 1119 .0 ug/1 PAP 03/03/2005 1119 1.0 ug/1 PAP 03/03/2005 1119 2.0 ug/1 PAP 03/03/2005 1119 Dilvl!:i & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2%48 / 81 r, E. Durst Avenue I Greenwood, SC 29049 I (864) ~29-44 lJ I Fax (864) 229-7119 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAcYIS FLWD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Certification Number: 25 Project Number: 61621.01 Report Date Page 59 of 88 April 18, 2005 Report ID: AC1040 QC Batch Report -Matrix Spikes and Duplicates WorkGroup: WG40487 Matrix GW/ChemW MS{MSD MS0S022810-04:40487 Prep Method MSD05022810-04:40487 Analtyical Method: SW846 82608 1,1,1-TRICHLOROETHANE so. 00 < 5. 00 56.42 ug/1 113 88-124 1,1,2-TRICHLOROETHANE 50.00 < 5. 00 46.35 ug/1 97 88-128 1,1-DICHLOROETHENE 50.00 < 5.00 49. 72 ug/1 99 71-130 1, 2-DI,CHLOROE'THANE 50.00 < 5. 00 55.40 ug/1 111 78-143 1,2-DICHLOROPROPANE 50.00 < 5.00 49. 31 ug/1 99 91-118 2-BUTANONE so.co < 10.00 56.52 ug/1 113 28-199 BENZENE 50.00 < 5.00 46.59 ug/1 93 77-123 CARBON TETRACHLORIDE 50.00 < 5.00 57.96 ug/1 116 63-135 CHLOROBENZENE SO.DO < 5.00 47.90 ug/1 96 78-123 CHLOROFORM 50.00 < 5.00 51. 43 ug/1 103 75-135 DIBROMOCHLOROMETHANE 50.00 < 5. 00 57. 33 ug/1 115 88-133 TETRACHLOROETHENE 50.00 < 5. 00 52. 91 ug/1 106 69-123 TOLUENE 50. 00 < 5 .00 48.66 ug/1 97 85-117 TRICHLOROETHENE 50. 00 < 5. 00 50.22 ug/1 100 75-121 VINYL CHLORIDE 50.00 < 10. 00 55.40 ug/1 111 47-136 1,1,1-TRICHLOROETHANE 50.00 55. 41 ug/1 111 2 15 88-124 1,1,2-TRICHLOROETHANE 50.00 48.64 ug/1 97 l 17 88-128 1,1-DICHLOROETHENE 50.00 46. 79 ug/1 94 6 17 71-13 0 1,2-DICHLOROETHANE 50.00 56. 19 ug/1 112 l 20 78-143 1,2-DICHLOROPROPANE 50.00 48. 49 ug/1 97 2 14 91-118 2-BUTANONE 50.00 61. 34 ug/1 123 a 31 28-199 BENZENE 50.00 45. 79 ug/1 92 2 17 77-123 CARBON TETRACHLORIDE 50.00 56 .23 ug/1 112 3 20 63-135 CHLOROBENZENE 50.00 47.08 ug/1 94 2 17 78-123 CHLOROFORM 50.00 so. 76 ug/1 102 l 17 75-135 DIBROMOCHLOROMETHANE 50.00 58.42 ug/1 117 2 15 88-133 TETRACHLOROETHENE 50.00 51. 90 ug/1 104 2 17 69-123 TOLUENE 50.00 47. 36 ug/1 95 3 15 85-117 TRICHLOROETHENE so.oo 48. 72 ug/1 97 3 17 75-121 VINYL CHLORIDE 50.00 52. 64 ug/1 105 5 19 47-136 NOTE1 MS/MSD \ recoveries are not evaluated if the sample concentration is greater than four times the spike added. Davis & Floyd, Inc. I PO Drawer 428 I Creenwood, SC 29fi48 j 81 I) E. Durst Avenue I Greenwood, SC 20(149 I (864) 229-4413 I Fax (864) 229-7119 ' , Df\YIS FLOYD LABORATORY ANALYSIS REPORT Client Contact TICONA, LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Cenijication Number: 25 Project Number: 61621.01 Report Date Page 60 of 88 April 18, 2005 Report ID: AC1040 QC Batch Report -Laboratory Control Standards and Duplicates WorkGroup: WG40487 Matrix GW/Chemw LCS LCS40487:1 Prep Method Analtyical Method: SW846 82608 1,1,1-TRICHLOROETHANE 20.00 20. 03 ug/1 100 79-127 1,1,2-TRICHLOROETHANE 20.00 20. 35 ug/1 102 83-143 1,1-DICH~ROETHENE 20.00 20.01 ug/1 100 63-141 1,2-DICHi.oROETHANE 20.00 22.57 ug/1 113 79-147 1, 2-.DICHLOROPROPANE 20.00 19.57 ug/1 98 86-130 2.-BUTANONE 20.00 22.01 ug/1 110 52-190 BENZENE 20.00 19. 55 ug/1 98 78-123 CARBON TETRACHLORIDE 20.00 20. 22 ug/1 101 58-132 CHLOROBENZENE 20.00 19. 89 ug/1 99 81-124 CHLOROFORM 20.00 20.82 ug/1 104 75-138 DIBROMOCHLOROMETHANE 20.00 21.27 ug/1 106 82-13 7 TETRACHLOROETHENE 20.00 20. 55 ug/1 103 71-12 0 TOLUENE 20.00 19 93 ug/1 100 81-121 TRICHLOROETHENE 20.00 19. 87 ug/1 99 76-120 VINYL CHLORIDE 20.00 20 51 ug/1 103 51-138 Davis & Floyd, Inc. I PO Drawer 42H I Greenwood, SC 2%48 I 816 E. Durst Avenue ! Gr(!Cnwood, SC 2%49 / (86.J) ~29-4413 I Fax (864) 229-7119 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I D~IS FLOYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Cenijication Number: 25 Project Number: 61621.01 Report Date Page 61 of ea April 18, 2005 Report ID: AC1040 QC Batch Report -Batch Sample List WorkGroup WG40388 D~scription: SV/8270/BNA/TCL SV/DOW Sample ID Client ID Run# L05022007-02 F-55 1 L0502200_7-02 F-55 2 MB4038_8·: 1 Method Blank 1 LCS40388:1 Laboratory Control Spike 1 MS05022007-02 :40388 Matrix Spike 1 MSD05022007-02:40388 Matrix Spike Duplicate 1 Matrix Prep Method GW/ChemW SW846 3510C Analtyical Method: SW846 8270C PREP ANALYTICAL Date Time Date Time 02/22/2005 0800 03/01/2005 1845 02/22/2005 0800 03/02/2005 1256 02/22/2005 0800 03/01/2005 1235 02/22/2005 0600 03/01/2005 1316 02/22/2005 0800 03/01/2005 1925 02/22/2005 0800 03/01/2005 2008 Analyst JRN JRN JRN JRN JRN JRN Dilution 10 1 1 I Davis & rluyd, Inc. I PO Drawer 428 I Creenwood, SC 21JM8 I 6161:. Dursl ,-\venue I Greenwood, SC 2964'.I I (8(>•!) 22()-4413 I Fax (864) 229-7119 DAYIS FLMD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Cenification Number: 25 Project Number: 61621.0l Report Date April 18, 2005 Page 62 of 88 Report ID: AC1040 QC Batch Report -Surrogates % Recovery WorkGroup: WG40388 L05022007-02 03/01/2005 1845 M840388: ~ 03/01/2005 1235 LCS40388:1 03/01/2005 1316 MS05022007-02 :40388 03/01/2005 1925 MSD05022007-02:40388 03/01/2005 2008 TBP 2,4,6-TRIBROMOPHENOL FBP 2-FLUOROBIPHENYL 2FP 2-FLUOROPHENOL NBZ NITROBENZENE-D5 PHL PHENOL-OS TPH TERPHENYL-D14 91 111 74 77 78 82 90 104 90 105 Matrix Prep Method GW/ChemW SW846 3510C Analtyical Method: SW846 8270C 81 74 1 73 98 61 77 97 61 ,o 48 0 90 29 2 64 87 90 55 56 0;1vis & Floyd, Inc. I PO Drawer 42B I Greenwoorl, SC 2~1648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (/3(,,!) 229-44B I r-,1x (8(;4) 229-71 I~ I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAYIS FLOYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem carter QC Batch Report -Method Blanks WorkGroup: WG40388 Blfnk MB40388:l Parameter Result Qual Semi volatile Organics SW846 8270C 1,2,4-TRICHLOROBENZENE ' 0. 010 1,2-DICHLOROBENZENE ' 0. 010 1, 3-DI,CHLOROBENZENE ' 0.010 1,4-DICHLOROBENZENE ' 0. 010 2,4,5-TRICHLOROPHENOL ' 0.010 2,4,6-TRICHLOROPHENOL ' 0.010 2,4-DICHLOROPHENOL ' 0. 010 2,4-DIMETHYLPHENOL ' 0.010 2,4-DINITROPHENOL ' 0.025 2,4-DINITROTOLUENE ' 0.010 2,6-DINITROTOLUENE ' 0.010 2-CHLORONAPHTHALENE ' 0.010 2-CHLOROPHENOL ' o. 010 2-METHYL-4,6-DINITROPHENOL ' o. 025 2-METHYLNAPHTHALENE ' o. 010 2-METHYLPHENOL ' o. 010 2-NITROANILINE ' o. 010 2-NITROPHENOL ' 0. 010 3,3'-DICHLOROBENZIDINE ' 0 .010 3-NITROANILINE ' 0. 010 4-BROMOPHENYL PHENYL ETHER ' 0.010 4-CHLOR0-3-METHYLPHENOL ' 0.010 4-CHLOROANILINE ' 0.010 4-CHLOROPHENYL PHENYL ETHER ' 0.010 4 -METHYLPHENOL ' 0. 010 4-NITROANILINE ' ~-010 4-NITROPHENOL ' 0.025 ACENAPHTHENE ' 0.010 ACENAPHTHYLENE ' 0.010 ANTHRACENE ' 0.010 BENZO(A)ANTHRACENE ' 0.010 BENZO(A)PYRENE ' 0.010 BENZO{B)FLUORANTHENE ' 0.010 BENZO{G,H,I)PERYLENE ' 0.010 BENZO(K)FLUORANTHENE ' 0. 010 BENZOIC ACID ' 0. 050 NC Certification Number: 25 Project Number: 61621.01 Report Date Page 63 of 88 Matrix: GW/ChemW RDL Units 0.010 mg/1 0 .010 mg/1 0 .010 mg/1 0 .010 mg/1 0 .010 mg/1 0. 010 mg/1 0 .010 mg/1 0 .010 mg/1 0 .025 mg/1 0. 010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0.025 mg/1 0. 010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0. 010 mg/1 0.010 mg/1 0.010 mg/1 0,010 mg/1 o. 010 mg/1 0 010 mg/1 0. 010 mg/1 0 .025 mg/1 0 .010 mg/1 0 .010 mg/1 0.010 mg/1 0 .010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0.050 mg/1 April 18, 2005 Report ID: AC1040 Analyst Date JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 Time 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 I Davis & Floyd, Inc. I PO Drawer 41.H I Creenwood, SC 2964B I H 16 I:. Durst Avenue I Greenwood, .SC 2%4(J I (8G4) :!.:!.9-4413 I Fax (864) 229-7119 DAYIS FLOYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter QC Batch Report-Method Blanks WorkGroup: WG40388 Blfnk MB40388:l Parameter Result Qual BENZYL ALCOHOL ' 0.010 BIS(2-CHLOROETHOXY)METHANE ' 0.010 BIS(2-CHLOROETHYL)ETHER ' 0.010 BIS(2-CHLOROISOPR0PYL)ETHER ' 0.010 BIS(2-~HYLHEXYL)PHTHALATE ' 0.010 BUTYL BENZYL PHTHALATE ' 0. 010 CHRYSENE ' 0.010 D1-N-BUTYL PHTHALATE ' 0.010 DI-N-OCTYL PHTHALATE ' 0.010 DIBENZ(A,H)ANTHRACENE ' 0. 010 DIBENZOFURAN ' 0.010 DIETHYL PHTHALATE ' 0.010 DIMETHYL PHTHALATE ' 0. 010 FLUORANTHENE ' 0.010 FLUORENE ' 0.010 HEXACHLOROBENZENE ' 0.010 HEXACHLOROBUTADIENE ' 0.010 HEXACHLOROCYCLOPENTADIENE ' 0.010 HEXACHLOROETHANE ' 0. 010 INDENO(l,2,3-CD)PYRENE ' 0.010 ISOPHORONE ' 0.010 N-NITROSODI-N-PROPYLAMINE ' 0. 010 N-NITROSODIPHENYLAMINE ' 0.010 NAPHTHALENE ' 0.010 NI TROBENZENE ' 0. 010 PENTACHLOROPHENOL ' 0.025 PHENANTHRENE ' 0.010 PHENOL ' o .. 010 PYRENE ' 0.010 SW846 8270C DOWI'HERM 1,1'-BIPHENYL ' 0. 010 BIPHENYL ETHER ' 0.010 NC Certification Number: 25 Project Number: 61621.01 Report Date Page 64 of 88 Matrix: GW/ChemW RDL Units 0.010 mg/1 0. 010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0. 010 mg/1 0. 010 mg/1 0. 010 mg/1 0. 010 mg/1 0. 010 mg/1 0.010 mg/1 0. 010 mg/1 0.010 mg/1 0 010 mg/1 0 010 mg/1 0. 010 mg/1 o. 010 mg/1 0 010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0.025 mg/1 0.010 mg/1 0. 010 mg/1 0. 010 mg/1 0 010 mg/1 0.010 mg/1 April 18, 2005 Report ID: AC1040 Analyst Date JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 Time 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 Davis &-floyrl, Inc. I PO DrJwer 428 Creenwood, SC 29648 I 816 E. Durst Avenue I Creenwund, SC 29649 I (B64) 229-441 J I F,ix (864) L.29-7 l 19 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAYIS FLbYD Client Contact LABORATORY ANALYSIS REPORT TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pcm Carter NC Certification Number: 25 Project Number: 61621.01 Report ~ate Page 65 of 88 April 18, 2005 Report ID: AC1040 QC Batch Report -Method Blanks WorkGroup: WG40388 Matrix: GW/ChemW Blank MB403881l Prep Procedure Method Analyst Prep Date Analytical Prep Procedures: DOWTHERM SW846 35008 DBC 02/22/2005 0800 82?0 SVOC PREP SW846 3510C DBC 02/22/2005 0800 I Davis S, Floycl, Inc. I 1-'0 Drawer 42H I Creenwnl)d, SC 2%4B I 816 E. Durs! Avenue I Gree11wuod, SC 2%•i9 I (Hfi ... +J 229-441 :I I F.ix (1364) 229-71 19 DAYIS FLOYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Cenijication Number: 25 Project Number: 61621.01 Report Date Page 66 of 88 April 18, 2005 Report ID: AC1040 QC Batch Report -Matrix Spikes and Duplicates WorkGroup: WG40388 M1/MSD 1,2,4-TRICHLOROBENZENE 1,4-DICHLOROBENZENE 2,4-DINITROTOLUENE 2 -CHLO,RONAPHTHALENE 2-CHLOROPHENOL 2-NITROPHENOL 4 -BROMOPHENYL PHENYL ETHER 4-CHLOR0-3-METHYLPHENOL 4-NITROPHENOL ACENAPHTHENE DI-N-OCTYL PHTHALATE N-NITROSODI-N-PROPYLAMINE PENTACHLOROPHENOL PHENOL PYRENE 1,2,4-TRICHLOROBENZENE 1,4-DICHLOROBENZENE 2,4-DINITROTOLUENE 2-CHLORONAPHTHALENE 2-CHLOROPHENOL 2-NITROPHENOL 4 -BROMOPHENYL PHENYL ETHER 4-CHLOR0-3-METHYLPHENOL 4 -NI TROPHENOL ACENAPHTHENE DI-N-OCTYL PHTHALATE N-NITROSODI-N-PROPYLAMINE PENTACHLOROPHENOL PHENOL PYRENE MS05022007-02:40388 MSD05022007-02:40388 0.0500 0 .0500 0 . 0500 0. 0500 0 .0750 0.0750 0.0500 0.0750 0.0750 0.0500 0.0500 0.0500 0.0750 0.0750 0.0500 0 .0500 0 .0500 0 .0500 0 .0500 0.0750 0.0750 0.0500 0.0750 0.0750 o.osoo 0.0500 0. 0500 0.0750 0.0750 0.0500 NOTB1 MS/MSD t recoveries are not evaluated if the < 0 .0100 < 0 . 0100 < o . 0100 < 0 .0100 < 0 .0100 < 0.0100 < 0.0100 < 0.0100 < 0.0250 < 0.0100 < 0.0100 < 0.0100 < 0 . 0250 0 .340 < o. 0100 0.0189 0. 0392 0.0100 0.0100 0.0808 0.0100 0.0351 0.110 0. 0592 0.0100 0.0195 0 .155 0.0521 0. 433 0.0409 Matrix Prep Method GW/ChemW SW846 3510C Analtyical Method: SW846 8270C 0.0235 mg/1 47 0.0309 mg/1 62 0.0318 mg/1 64 0 .0100 mg/1 5 0 .0764 mg/1 102 0. 0100 mg/1 3 0 . 0341 mg/1 68 0. 0906 mg/1 121 0.0250 mg/1 7 0.0100 mg/1 15 0.0190 mg/1 38 0.165 mg/1 81 0.0556 mg/1 74 0 .418 mg/1 105 0.0388 mg/1 78 mg/1 38 22 mg/1 78 ,. mg/1 0 200 mg/1 • 18 mg/1 108 6 mg/1 0 200 mg/1 70 3 mg/1 147 19 mg/1 79 166 mg/1 0 200 mg/1 39 3 mg/1 62 6 mg/1 69 7 mg/1 125 3 mg/1 82 5 sample concentration is greater than four times 33-92 30-86 45-107 70-130 34-95 70-130 70-130 35-110 16-88 41-107 70-130 36-106 32-126 4-83 51-132 30 33-92 20 30-86 22 45-107 20 70-130 29 34-95 20 70-130 20 70-130 22 35-110 28 16-88 26 41-107 20 70-130 22 36-106 38 32-126 28 4-83 24 51-132 the spike added. D;:wis & Floyd, Inc. I PO Drawer 42f:I I Grr!enwond, SC 29(AH I I.I! r) E. Durst Avenut~ I Greenwood, SC 2%49 I (H(14) 229-4413 I Fax (Bti4) 229-71 19 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAYIS FL6YD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Cenification Number: 25 Project Number: 61621.01 Report Date Page 67 of 88 April 18, 2005 Report ID: AC1040 QC Batch Report -Laboratory Control Standards and Duplicates WorkGroup: WG40388 Lq, LCS40388:1 1,2,4-TRICHLOROBEN~ENE 0.0500 1,4-DICHLOROBENZENE 0.0500 2,4-DINI!ROTOLUENE 0.0500 2-CHLORONAPHTHALENE 0.0500 2-CHLOROPHENOL 0.0750 2-NITROPHENOL 0.0750 4-BROMOPHENYL PHENYL ETHER 0.0500 4-CHLOR0-3-METHYLPHENOL 0.0750 4-NITROPHENOL 0.0750 ACENAPHTHENE 0.0500 DI-N-OCTYL PHTHALATE o. 0500 N-NITROSODI-N-PROPYLAMINE 0. 0500 PENTACHLOROPHENOL 0 0750 PHENOL 0. 0750 PYRENE 0.0500 0.0333 0.0308 0. 0455 0.0374 0. 0547 0.0612 0.0383 0.0661 0.0435 o. 0410 0 .0565 0 . 0456 0 . 0339 0.0426 0.0459 Matrix Prep Method GW/ChemW SW846 3510C Analtyical Method: SW846 8270C mg/1 67 30-91 mg/1 62 29-83 mg/1 91 46-108 mg/1 75 60-118 mg/1 73 29-106 rng/1 82 49-111 mg/1 77 61-111 mg/1 88 34-110 mg/1 58 4-80 mg/1 82 39-109 mg/1 113 59-111 mg/1 91 36-114 mg/1 45 20-102 mg/1 57 2-83 mg/1 92 55-126 Davis & Floyd, Inc. I PO Drawer 428 I C1eenwood, SC 29648 I H 16 E. Durst Avenue I Crcenwood, SC 2964~) I {864) 229-44 U I Fax (864) 229-7"1 19 DAYIS FLtTYD LABORATORY ANALYSIS REPORT Sample ID L05022303-01 L05022303-02 LOS022,i03-03 L05022303-04 L05022812-01 Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Certification Number: 25 Project Number: 61621.01 Report Date Page 68 of 88 April 18, 2005 Report ID: AC1040 QC Batch Report -Batch Sample List WorkGroup WG40471 D~scription: SV/8270/BNA/TCL SV/DOW Client ID Run# PEW-1 1 PEW-3 PEW-4 1 DUP-4 1 FB-01 1 Matrix Prep Method GW/ChemW SW846 3510C Analtyical Method: SW846 8270C PREP ANALYTICAL Date Time Date Time 02/28/2005 0800 03/03/2005 1238 02/28/2005 0800 03/03/2005 1515 02/28/2005 0800 03/03/2005 1557 02/28/2005 0800 03/03/2005 1636 02/28/2005 0800 03/03/2005 1715 Analyst JRN JRN JRN JRN JRN Dilution Davi:-& Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst 1\venue I Greenwood, SC 29649 I (864) 229-4413 I Fax (864) 229-71 19 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAYIS FLtJYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Certification Number: 25 Project Number: 61621.01 Report Date April 18, 2005 Page 69 of BB Report ID: AC1040 QC Batch Report -Surrogates % Recovery WorkGroup: WG40471 Matrix GW/ChemW Prep Method SW846 3510C Analtyical Method: SW846 8270C L05022303-01 03/03/2005 1238 45 42 36 44 29 105022303-02 03/03/2005 1515 83 84 63 83 52 L050223·o·3-03 03/03/2005 1557 80 59 46 60 39 L05022303-04 03/03/2005 1636 " 78 65 81 50 105022812-01 03/03/2005 1715 77 63 52 68 42 TBP 2,4,6-TRIBROMOPHENOL FBP 2-FLUOROBIPHENYL 2FP 2 -FLUOROPHENOL NBZ NITROBENZENE-D5 PHL PHENOL-OS TPH TERPHENYL-D14 44 77 86 83 74 I Davis & Floyd, Inc. I PO Drawer 420 I Creenwond, SC 29648 I 816 E. Durst Avcmu! I Creenwoorl, SC 29fi49 I WM) 229-4413 I Fax (1164) 229-71 19 Di\YIS FLOYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Certification Number: 25 Project Number: 61621.01 Report Date Page 70 of 88 April 18, 2005 Report ID: AC1040 QC Batch Report -Batch Sample List WorkGroup WG40388 Dercription: SV/8270/BNA/TCL SV/DOW Sample ID Client ID Run# L05022007-02 F-55 L05022007-02 F-55 2 MB4038W~ 1 Method Blank 1 LCS40388:1 Laboratory Control Spike MS05022007-02:40388 Matrix Spike 1 MSD05022007-02:40388 Matrix Spike Duplicate 1 Matrix Prep Method GW/Chemw SW846 35008 Analtyical Method: SW846 8270C DOWTHERM PREP ANALYTICAL Date Time Date Time Analyst 02/22/2005 0800 03/01/2005 1806 JRN 02/22/2005 0800 03/01/2005 1845 JRN 02/22/2005 0800 03/01/2005 1235 JRN 02/22/2005 0800 03/01/2005 1316 JRN 02/22/2005 0800 03/01/2005 1925 JRN 02/22/2005 0800 03/01/2005 2008 JRN Dilution 1000 1 1 1 Davis & Floyrl, Inc. I PO Drawer 428 j Greenwood, SC 29648 / 8 I 6 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-4413 I Fax (864) 229-7119 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAYIS FLiWD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem carter NC Certification Number: 25 Project Number, 61621.01 Report Date Page 71 of 88 April 18, 2005 Report ID: AC1040 QC Batch Report -Surrogates % Recovery WorkGroup: WG40388 L05022007-02 03/01/2005 MB40388:l 03/01/2005 LCS403!38:l 03/01/2005 MS05022007-02:40388 03/01/2005 MSD05022007-02:40388 03/01/2005 FBP -2-FLUOROBIPHENYL NOTB: *NE -Result was not evaluated. 1845 116 1235 81 1316 86 1925 •NE 2008 •NE Matrix Prep Method GW/Chemw SW846 3500B Analtyical Method: SW846 8270C DOWTHERM D;ivis & Floyrl, Inc. I PO Dr,1.wcr 42B I Gre1~nwood, SC 29,;,rn I 111 fi F.. Durst Ave11tll! I Gree11wnnd, SC 2%4'.J I (H64) 229-441 J I Fc1x WG4) 229~7119 DAYIS FL(WD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter QC Batch Report-Method Blanks workGroup: WG40388 B\ank MB403881l Parameter Result Qual Semi volatile Organics SW846 8270C 1,2,4-TRICHLOROBENZENE ' 0.010 1,2-DICHµ)ROBENZENE ' 0.010 1, 3-Dl,CHLOROBENZENE ' 0.010 1,4-DICHLOROBENZENE ' 0.010 2,4,5-TRICHLOROPHENOL ' 0.010 2,4,6-TRICHLOROPHENOL ' 0.010 2,4-DICHLOROPHENOL ' 0. 010 2,4-DIMETHYLPHENOL ' 0.010 2,4-DINITROPHENOL ' 0.025 2,4-DINITROTOLUENE ' 0.010 2,6-DINITROTOLUENE ' 0. 010 2-CHLORONAPHTHALENE ' 0.010 2-CHLOROPHENOL ' 0.010 2-METHYL-4,6-DINITROPHENOL ' 0.025 2-METHYLNAPHTHALENE ' 0.010 2-METHYLPHENOL ' 0.010 2-NITROANILINE ' 0.010 2-NITROPHENOL ' 0.010 3,3'-DICHLOROBENZIDINE ' 0.010 3-NITROANILINE ' 0. 010 4-BROMOPHENYL PHENYL ETHER ' 0. 010 4-CHLOR0-3-METHYLPHENOL ' 0.010 4-CHLOROANILINE ' 0.010 4-CHLOROPHENYL PHENYL ETHER ' 0.010 4-METHYLPHENOL ' 0.010 4-NITROANILINE ' 0.010 4-NITROPHENOL ' 0.025 ACENAPHTHENE ' 0.010 ACENAPHTHYLENE ' 0.010 ANTHRACENE ' o. 010 BENZO(A)ANTHRACENE ' 0.010 BENZO(A)PYRENE ' 0.010 BENZO(B)FLUORANTHENE ' 0.010 BENZO(G,H,I)PERYLENE ' 0.010 BENZO(K)FLUORANTHENE ' 0 010 BENZOIC ACID ' 0.050 NC Cenijication Number: 25 Project Number: 61621.01 Report Date April 18, 2005 Page 72 of 88 Report ID: AC1040 Matrix: GW/ChemW RDL Units Analyst Date Time 0.010 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 o. 010 mg/1 JRN 03/01/2005 1235 0 0l0 mg/1 JRN 03/01/2005 1235 0 .010 mg/1 JRN 03/01/2005 1235 0 .010 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 0.025 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 0.025 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 0. 010 mg/1 JRN 03/01/2005 1235 0. 010 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 0.025 mg/1 JRN 03/01/2005 1235 0. 010 mg/1 JRN 03/01/2005 1235 0 .010 mg/1 JRN 03/01/2005 1235 0. 010 mg/1 JRN 03/01/2005 1235 0. 0l0 mg/1 JRN 03/01/2005 1235 o. 010 mg/1 JRN 03/01/2005 1235 o. 010 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 0.010 mg/1 JRN 03/01/2005 1235 0.050 mg/1 JRN 03/01/2005 1235 Davis & Floyd, Inc. I PO Draw1:r 42H I Greenwood, SC 29648 I 8 l 6 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-4413 I F<1x (864) 229-7119 I I I I I I I I I I I I II I I I I I I I I I I I I I I I I I I I I I I I I I DA[IS FLOYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem carter QC Batch Report-Method Blanks WorkGroup: WG-10388 Bl~ank MB403881l Parameter Result Qual BENZYL ALCOHOL ' 0.010 818(2-CHLOROETHOXY)METHANE ' 0.010 818(2-CHLOROETHYL)ETHER ' 0.010 818(2-CHLOROISOPROPYL)ETHER ' 0.010 BIS (2-_E1°HYLHEXYL) PHTHALATE ' 0.010 BUTYL BENZYL PHTHALATE ' 0.010 CHRYSENE ' 0.010 DI-N-BUTYL PHTHALATE ' 0.010 DI-N-OCTYL PHTHALATE ' 0.010 DIBENZ(A,H)ANTHRACENE ' 0.010 DIBENZOFURAN ' 0.010 DIETHYL PHTHALATE ' 0.010 DIMETHYL PHTHALATE ' 0.010 FLUORANTHENE ' 0.010 FLUORENE ' 0.010 HEXACHLOROBENZENE ' 0.010 HEXACHLOROBUTADIENE ' 0 .010 HEXACHLOROCYCLOPENTADIENE ' 0. 010 HEXACHLOROETHANE ' 0 .010 INDENO(l,2,3-CD)PYRENE ' 0. 010 ISOPHORONE ' 0.010 N-NITROSOOI-N-PROPYLAMINE ' 0.010 N-NITROSODIPHENYLAMINE ' 0.010 NAPHTHALENE ' 0.010 NITROBENZENE ' 0.010 PENTACHLOROPHENOL ' 0.025 PHENANTHRENE ' 0.010 PHENOL ' 0.010 PYRENE ' 0.010 SW846 8270C DOWTHERM 1,1'-BIPHENYL ' 0 .010 BIPHENYL ETHER ' 0.010 NC Certification Number: 25 Project Number: 61621.01 Report Date Page 73 of BB Matrix: GW/Chemw RDL Units 0. 010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0 010 mg/1 0.010 mg/1 0. 010 mg/1 0. 010 mg/1 0. 010 mg/1 0.010 mg/1 0. 010 mg/1 0.010 mg/1 0. 010 mg/1 0.010 mg/1 0. 010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0.010 mg/1 0. 010 mg/1 0. 025 rng/1 0.010 mg/1 0. 010 mg/1 0. 010 mg/1 0.010 mg/1 0.010 mg/1 April 18, 2005 Report ID: AC1040 Analyst Date JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2.005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 JRN 03/01/2005 Time 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 1235 Davis & Floyd, Inc. I PO Drawer 428 j Grei:nwood, SC 29(148 I 816 E. Durst Avenue I Greenwood, SC 2%49 I (864) 229-4413 j Fax (864) 229-71·19 DAYIS FLbYD Client Contact LABORATORY ANALYSIS REPORT TICONA, LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Certification Number: 25 Project Number: 61621.01 Report Date April 18, 2005 Page 74 of 88 Report ID: AC1040 QC Batch Report -Method Blanks WorkGroup: WGt0388 Matrix: GW/ChemW Bl:ank MB403881l Prep Procedure Method Analyst Prep Date Analytical Prep Proceduresz DOWTHERM SW846 35008 DBC 02/22/2005 0800 8270 svoc PREP SW846 3510C DBC 02/22/2005 0800 Davis~~ Floyd, lnc. ) 1-'0 Drawer 42H I Creenwond, SC 29(l48 I 81 (, I:. Durst Avenue I Greenwood, SC 29(,49 I (864) 22:J-44I J I fax (8(i4) 2n-7 I 1 '.J I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAYIS FLMD LABORATORY ANALYSIS REPORT 1,1'-BIPHENYL BIPHENYL ETHER 1,1'-BIPHENYL BIPHENYL ETHER Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem carter NC Certification Number: 25 Project Number: 61621.01 Report Date Page 75 of 88 April 18, 2005 Report ID: AC1040 QC Batch Report -Matrix Spikes and Duplicates WorkGroup: WG40388 MS/MSD MS05022007-02:40388 MSD05022007-02:40388 o.osoo 0.0500 0.0500 0.0500 Matrix Prep Method GW/ChemW SW846 35008 Analtyical Method: SW846 8270C DOWTHERM Not Evaluated See Note Below. Not Evaluated See Note Below. Not Evaluated See Note Below. Not Evaluated See Note Below. NOTE: MS/MSD t recoveries are not evaluated if the sample concentration is greater than four times the spike added. Davis & Floyd, Inc. I PO Drawer 428 I Creenwnod, SC 2964B I 816 E. Durst Avenue I Creenwood, SC 29fi49 I (864) 229-4413 I Fax (864) 229-71 !9 DAYIS FLMD LABORATORY ANALYSIS REPORT 1,1'-BIPHENYL BIPHENYL ETHER Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Fem Carter NC Cenification Number: 25 Project Number: 61621.01 Report Date April 18, 2005 Page 76 of 88 Report ID: AC1040 QC Batch Report -Laboratory Control Standards and Duplicates WorkGroup: WG40388 LCS LCS403881l 0.0500 0.0500 0.0398 0.0388 Matrix Prep Method GW/Chemw SW846 35008 Analtyical Method: 8WB46 8270C OOWTHERM mg/1 mg/1 80 78 40-108 42-109 Davis & Floyrl, Inc. I PO Druwer 428 I Creenwood, SC 29b48 I 81 (i E. Durst Avenue I Creenwood, SC 2%4~J I (8(14) 22'.l-441 J I Fa;,,: iH64) 229-71 19 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAVIS Fibito LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem carter NC Cenijication Number: 25 Project Number, 61621.01 Report Date April 18, 2005 Page 77 of BB Report ID: AC1040 QC Batch Report -Batch Sample List WorkGroup WG40471 Matrix GW/ChemW □e._scription: SV/8270/BNA/TCL SV/DOW Prep Method SW846 3500B Analtyical Method: SW846 8270C DOWTHERM PREP ANALYTICAL Sample ID Client ID Run# Date Time Date Time Analyst LOS022303-01 PEW-1 1 02/28/2005 0800 03/03/2005 1238 JRN L05022303-02 PEW-3 02/28/2005 0800 03/03/2005 1438 JRN L05022_303-02 PEW-3 2 02/28/2005 0800 03/03/2005 1756 JRN L050223 03-03 PEW-4 1 02/28/2005 0800 03/03/2005 1557 JRN L05022303-04 DUP-4 1 02/28/2005 0800 03/03/2005 1636 JRN L05022812-01 FB-01 1 02/28/2005 0800 03/03/2005 1715 JRN MB40471:l Method Blank 1 02/28/2005 0800 03/03/2005 1005 JRN LCS40471:l Laboratory Control Spike 1 02/28/2005 0800 03/03/2005 1530 JRN MS05022303-01:40471 Matrix Spike 1 02/28/2005 0800 03/03/2005 1319 JRN MSD05022303-01:40471 Matrix Spike Duplicate 1 02/28/2005 0800 03/03/2005 1359 JRN Dilution 1 4 10 1 1 1 1 1 Davis & Fluyd, !nc. I PO Drawer 42B I Greenwood, SC 2%48 I fl 16 E. Our~t Avenue I Greenwood, SC 2~h-l9 I (864) 229-4413 I F;.ix (864) 229-71 19 DAYIS FLtrYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Cenijication Number: 25 Project Number: 61621.01 Report Date Page 78 of as April 18, 2005 Report ID: AC1040 QC Batch Report -Surrogates % Recovery WorkGroup: WG40i71 L05022303-01 03/03/2005 L05022303-02 03/03/2005 L05022,303-03 03/03/2005 L05022303-04 03/03/2005 L05022812-01 03/03/2005 MB40471:l 03/03/2005 LCS40471:l 03/03/2005 MSOS022303-0l:40471 03/03/2005 MSD05022303-0l:40471 03/03/2005 FBP -2-FLUOROBIPHENYL 1238 43 1438 93 1557 60 1636 79 1715 64 1005 78 1530 78 1319 80 1359 83 Matrix Prep Method GW/ChemW SW846 35008 Analtyical Method: SW846 8270C DOWTHERM Davis & Floyd, Inc. I PO Dr;-iwer· 4:!U I Grecnwr.iud, SC 2%48 I 81 () E. Durst Ave;nuL' I Grec11w1Jod, SC 1')h49 I (864) 229-441 :\ I Fax (Hf.4) 229-7119 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DA~IS FLMD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter QC Batch Report -Method Blanks WorkGroup: WGt0•71 Blpnk MB404711l Parameter Semivolatile Organics SW846 8270C DOWTHERM 1, l' -BI PHENYL 2,3-DIHYDROXYBIPHENYL BIPHENYL ETHER Prep Procedure Analytical Prep Procedures: Method ' ' ' DOWTHERM SW846 3500B Result Qual 0 .010 0 .025 0 .010 Analyst DBC NC Certification Number: 25 Project Number: 61621.01 Report Date Page 79 of 88 Matrix: GW/ChemW RDL Units 0.010 mg/1 0. 025 mg/1 0. 010 mg/1 Prep Date 02/28/2005 0800 April 18, 2005 Report ID: AC1040 Analyst JRN JRN JRN Date Time 03/03/2005 1005 03/03/2005 1005 03/03/2005 1005 Davis & Floyd, Inc I PO Drawer 42S I Greenwood, SC 29648 I 816 E. Dur.sr Avenue I Creenwo<>d, SC 29649 I (Hf>4) 229-4413 I Fax (864) 229-7 ! 19 DAVIS FLij-YD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Cenijication Number: 25 Project Number: 61621.01 Report Date Page BO of 88 April 18, 2005 Report ID: AC1040 QC Batch Report -Matrix Spikes and Duplicates WorkGroup: WG40471 M~/MSD MS05022303-0l:40471 1,1'-BIPHENYL 2,3-DIHYDROXYBIPHENYL BIPHENYL ETHER 1,1'-BIPHENYL 2,3-DIHYDROXYBIPHENYL 8 I PHENYL ETHER NOTS: MS/MSD l recoveries MSD05022303-01140471 are not evaluated 0.0500 0.100 0.0500 0.0500 0 .100 0.0500 if the Matrix Prep Method GW/ChemW SW846 35008 Analtyical Method: SW846 8270C DOWTHERM < 0.0100 < 0 0250 < 0 0100 0. 04 03 0.0250 0 0388 0.0382 0.0250 0.0364 mg/1 mg/1 mg/1 sample concentration is mg/1 mg/1 mg/1 81 0 78 greater than 76 0 73 5 0 6 four times 34-102 18-125 31-110 JO 15 31 34-102 18-125 31-110 the spike added. Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 ) 8 ! 6 E. Durst Avenue / Greenwood, SC 29649 I (86-t) 229-4413 I F;1x {864) 229-7119 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Certification Number: 25 Project Number: 61621.01 Report Date April 18, 2005 Page Bl of 88 Report ID: AC1040 QC Batch Report -Laboratory Control Standards and Duplicates WorkGroup: WG40471 L~S LCS404711l 1,1'-BIPHENYL 2,3-DIHYDROXYBIPHENYL BI PHENYL ETHER o.osoo 0.100 0.0500 0.0376 0. 0711 0.0360 Matrix GW/ChemW Prep Method SW846 3500B Analtyical Method: SW846 8270C DOWTHERM mg/1 mg/1 mg/1 75 71 72 40-108 39-103 42-109 Davis & Floyd, Inc. j PO Drawer 42.rJ I Creenwood, SC 29648 I 816 F.. Durst Avenue I Crcenwood, SC 2%4:J I (8(i4) 229-•l4 I 3 I Fax (a64) 229-71 ! 9 DAYIS FLOYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Cenijication Number: 25 Project Number: 61621.01 Report Date April 18, 2005 Page 82 of 98 Report ID: AC1040 QC Batch Report -Batch Sample List WorkGroup WG40535 Matrix GW/ChemW De,scription: TOC GW Prep Method Analtyical Method: SW846 9060 ANALYTICAL Sample ID Client ro Run# PRBP Date Time Date ·Time Analyst Dilution L05022401-0l V-23 L05022401-02 K-28 MB4053?:: 1 Method Blank MB40535:2 Method Blank LCS40535:l Laboratory Control Spike LCS4053S:2 Laboratory Control Spike MS05022402-02 40535 Matrix Spike MS05022407-05:40535 Matrix Spike MS005022402-02:40535 Matrix Spike Duplicate MSD05022407-05:40535 Matrix Spike Duplicate 03/03/2005 2002 1 03/03/2005 2027 1 03/03/2005 2327 1 03/04/2005 0435 1 03/03/2005 2255 1 03/04/2005 0404 1 03/03/2005 2205 1 03/04/2005 0311 1 03/03/2005 2223 1 03/04/2005 0328 CDC CDC CDC CDC CDC CDC CDC CDC CDC CDC 1000 25 1 1 1 1 Davis & Floyd, lnc. I PO Dr;iwer 4211 I Creenwnod, SC 2%48 I 816 E. Durst /\venue I Greenwood, SC 29649 I (B64) 22';.l-441 J I Fax (864) 229-711 1) I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I D_AYIS FLOYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 29152 Pem Carter QC Batch Report -Method Blanks Parameter Wet Chemistry SW846 9060 WorkGroup: WG40535 B\ank MB405351l ORGANIC CARBON, TOTAL Result Qual < a.so NC Certification Number: 25 Project Number: 61621.01 Report Date Page 83 of 88 Matrix: GW/ChemW RDL units April 18, 2005 Report ID: AC1040 Analyst Date Time 0.50 CDC 03/03/2005 2327 Davis & Floyd, Inc. I PO Dr,1wer 42B I Creenwood, SC 29648 I 816 E. Durst Avcttue I Greenwnocl, SC 29649 I (864) 219-4413 I Fax (864) 229~7 I 'I 'J DAYIS FLMD LABORATORY ANALYSIS REPORT Client Contact• TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter QC Batch Report -Method Blanks Parameter Wet Chemistry SW846 9060 WorkGroup: WG40535 B~ank MB40535:2 ORGANIC CARBON, TOTAL Result Qual < 0.50 NC Cenijication Number: 25 Project Number: 61621.01 Report Date Page 84 of 88 Matrix: GW/Chemw RDL Units April 18, 2005 Report ID: AC1040 Analyst Date Time 0.50 mg/1 CDC 03/04/2005 0435 Dew is & Floyd, Inc. I PO fk1wer 42H I Greenwond, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-44 l 3 I Fax (864) 229-7119 I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAllS FLOYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Cenification Number: 25 Project Number: 61621.01 Report Date April 18, 2005 Page 85 of 88 Report ID: AC1040 QC Batch Report -Matrix Spikes and Duplicates WorkGroup: WG40535 Matrix GW/Chemw MS{MSD MS05022402-02:40535 Prep Method MSD05022402-02:40535 Analtyical Method: SW846 9060 ORGANIC CARBON, TOTAL 10.00 6.69 17.00 mg/1 103 74-125 ORGANIC CARBON, TOTAL 10.00 16.50 98 3 11 74-125 I NOTB: MS/MSD % recoveries are not evaluated if the sample concentration is greater than four times the spike added. I I I I I I I I I D,1vic-,~ Floyrl, Irie. I r'O Drawer 42B I Gt"(::enwood, SC 2~164B I 816 E. Durst Avenue I Greenwood, SC 2':)b49 I (864) 229-441 J I F<tx (864) 229-7119 DAYIS FL(JYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Certification Number: 25 Project Number: 61621.01 Report Date Page 86 of 88 April 18, 2005 Report ID: AC1040 QC Batch Report -Matrix Spikes and Duplicates WorkGroup: WG40535 Matrix GW/ChemW MS{MSD MS05022407-05140535 Prep Method MSD05022407-05:40535 Analtyical Method: SW846 9060 ORGAN"IC CARBON, TOTAL 10.00 1. 66 12.20 105 74-125 ORGANIC CARBON, TOTAL 10.00 11. 80 mg/1 101 3 11 74-125 NOTB: MS/MSD \ recoveries are not evaluated if the sample concentration is greater than four times the spike added. Dc1vis & Floyd, Inc. I PO Dr,1wer 42/l I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-4413 I Fax (864) 229-71 ·1 9 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAYIS FLtfYD LABORATORY ANALYSIS REPORT Client Contact TICONA, LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Certification Number: 25 Project Number: 61621.01 Report Date April 18, 2005 Page 87 of 88 Report ID: AC1040 QC Balch Report -Laboratory Control Standards and Duplicates workGroup: WG40535 Matrix GW/ChemW LCf LCS40535:l Prep Method Analtyical Method: SW846 9060 ORGANIC CARBON, TOTAL 25.00 9.92 mg/1 99 90-110 O;,vis &.· Floyd, Inc. I PO Drawer 428 \ Creenwood, SC 29648 I 816 E. Durst Awnue I Gret.'nwoorl, SC 29649 I (B64) 22<J-4413 I F,ix (864) 229-71 I 9 Df\YIS FLOYD LABORATORY ANALYSIS REPORT Client Contact TICONA,LLC 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Pem Carter NC Cenification Number: 25 Project Number: 61621.01 Report Date April 1B, 2005 Page 88 of 88 Report ID: AC1040 QC Batch Report -Laboratory Control Standards and Duplicates WorkGroup: WG40535 Matrix GW/ChemW LCf LCS4053512 Prep Method Analtyical Method: SW846 9060 ORGANIC CARBON, TOTAL 25.00 9.96 mg/1 100 90-110 D:wis & Floyd, Inc. I f'O Drawer 4.'.rn I Cree11woocl, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29()49 I (Rfi4) 229-4--113 I F:i.x (864) 22~)-7! 1 Y I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I D\YIS FLOYD LABORATORY ANALYSIS REPORT Method Conformance Summary Client: Ticona, LLC Project Number: 61621.01 Login(s): L0502 l 803, L0502 l 805, L050022007, L0502303, L05022401, L05022812 Report Date: April 18, 2005 Criteria Volatiles Sample Holding Time ✓ Standards Preparation ✓ Instrument Tuning ✓ Instrument Calibration ✓ Calibration Verification ✓ Degradation Check NIA Interference NIA Sample/Standard Blanks Results ✓ Method Accuracy • Method Precision ✓ Surrogate Recovery ✓ PDS/SD/MSA NIA TCLP Preparation NIA ✓ NIA Method Criteria Met Not Applicable 1,4-Semi Dioxane Volatiles ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ NIA NIA NIA NIA ✓ ✓ ✓ • ✓-• ✓ • NIA NIA NIA NIA * Method Criteria Not Met -See footnote(.,) below. PDS = SD = MSA= Post Digestion Spike · Serial Dilution Method of Standard Additions TOC ✓ ✓ NIA ✓ ✓ NIA NIA ✓ ✓ ✓ NA NIA NIA Footnotes: Volatiles-1,2-Dichloropropane on WG40376 exceeded the established lower limit of91 % (85 and 90) for the MS and MSD respectively). The LCS associated with this batch recovered within acceptable limits. Semivolatiles -Includes Dowtherm. Semivolatiles-Surrogates on WG40388 exceeded the established limit for FBP, 2FP and PHL. Multiple matrix spike failures were present in the MS and MSD. All failures are associated with sample L05022007-02 indicating a sample matrix interference. Surrogate recoveries for the method blank and LCS were within established limits. I Davis,, Floyd. Inc. I F'O Drawer 428 I Creenwood, SC 29648 I 816 E. Durst ,\venue I Creenwr.,nd, SC 296-19 I (864) 229-4413 I Fax (8641 229-71 I 9 ~ ~y Chain of Custody Record ClientJ::-.'tJ$1t. / .,,,,.,, _ J, _,, . . -1vl;L f,:1ffuC:1A-'i?S- Address r;:;_ ,0 <.3a)( §r:fJ.i/7 CUy 5'. (j) /A-< J!fcVVttiC I State 1 Zip Co<je JL ~txfc,• Project Name C;v4-/T7[,ru(J- Project No. , P.O. No. .2 &-.? t(}.J ;s---- Sample ID I Description Date (Containers for each sample may be combined on one line.) SHEALY ENVIRONMENTAL SERVICES, INC. 136 Vantage Point Drive Cayce, South Carolina 29033 Telephone No. (803) 791-9700 Fax No. (803) 791-9111 Report to Contact Te'::Jlp}ne No. I Fax No. I E-mail , /J'4f/ -:J2--;2 fl, ,t.J3,p__ •. '&,y/-'/ t-2 _yt('lll ,J · 9f.2. ,r .J<-19 Waybill No. I Quote No. Page l D/ Sampie,'s S:J:?tu,e ' L ~ ·--,. ,. Analysis (Attach list if more space is needed.) l x./ '"7/_ . Printed' .. t:.--nt:trc!J2 1 ';. /:-iNJ,'t,,+,,,_ _; ~~ No. of Containers Lot No. r§ 1 Matrix by Preserv<:-tive Type t,? ~ i " ~ . nme ~o ~ ... 5 s ~ 8 1, ~ .,. il •• § ~ ~ ~ 8 ~ ~ :z: ~ ~ ~ Remarks I Cooler /.0. ' a L l V-13 Z/23/,;i-09f-< ~ X 3 I X X _t;-~'7¾:k-cP-f).,,7-_ )::-Jf ¾ii,; )71-< t-X 1 I ·-,f2rfl /Jtkufi -I 'l/4,{1,..-09a, / X 2 J ,,.,...---·) /) Sample Disposal )( X K 1r :Jt;t;sS-- li:-Pr-p.reu-·t'zyt: ttJm\ ,fr IJc /, N.\.2., S z_{; 5 'ffie-,1s""c 2.1l1Lc' I < -.~c_ /4.-~t,tl,--;T 0,:.1 2.:::.v,4 f:tqj1:.iJ2:'J /i' -'l s ,t,.,) f 9 r-.is:) Note: All samples are retained for six weeks from receipt POSSible Haz7□ntificati~Ij □ Non-Haza □ Flamr,(able □ sLtant/~ Poison □ Unknown □ Retum to Client fDisposal by Lab unless other arrangements are made. Tu~ A':;:IJ1~fred (Prio_r iap/f required for expedited TAT.) ' QC Requirements (Specify) !.NeL "X 1uStan ush(~ ( 1. ~ . edby .',h c,(' --D~/2.✓.i-Time _ 1.Raceivedb~ ,.L J / J :J.-2]()_') Time / ~· r't2..J l{;,2S ,,,,,,,...,. .,._., / -It; 2 \ ,--"'fc/ -,:/ fl_A,,,A I 2.~-7~ ltlate ;;2-23-0S T7~_s 2. Received by Date Time 3. Relinquished by Date Time 3. Labr;'';;","s~by hL-" (/1 j I Data Time ,( 1.r{tJ ,:;-17~s-Commenrs LAB USE ONLY ,J Received on ice (Circ/e{;;;)No Ice Pack Receipt Temp. "C -- - --- ~-- -- -------SHEALY ENVIRONMENTAL SERVICES, INC. sey Chain of Custody Record 106 Vantage Point Drive Cayce, South Carolina 29033 Telephone No. (803) 791-9700 Fax No. (803) 791-9111 , Client r-,_,. ~ /' 7!2 /t( Report ~ntact J:l-611.. /J Te/epf]one ~Fax '3'fj:-mail ~ ~ . Quote No. ',, -ft/ . {, Jd"t /,fJeT '--6fUZ) .../tPf·-· _7.9 'fo / ;t;-'/:2 ,r.?£~ ~ , Address,H) }!, tJ ;( <fi1Jt;7 Sampler's/ignat~~. ~ _ Waybill No. / Pa:J.;_f,_ of j_ Cily {, (J ,~r l~ul> ~/, /l-, Analysis (Attach list if more space is needed.) -I _ 11'1 '([/;Jf/1,t.[-,. Project Name C~4 /T;'tu-vA--t)t&,4"] 'T. /tft,41,liJL, V, Project No. J6&-:.S1J PO. No. ~ No. of Containers ),/i'f$;:-_& Lot No. o• Matrix by Presen.;ative Type ~ ,'(~~ ·.\: G~ t Sample ID I Description Date Time "0 ~ ~ ~ ; I~ i5 ~ -;!_ '7 ~ ~" 1 ~ ~1 (Containers for each sample may be combined on one line.) ~ ~ ~ ! ~ ~ ~ ~ Remarks I Cooler ID. ' ' •'P_,,Sk l(f,;/,. tflo / X ? I')( -~e-r 7;4¢.c!il~ .., f-,_s:-5" I .c,~· l ( X x )< 1f")'t.4JJiJ ,tr, ~i~ \)) -6 -,J'11/? 'iJ L/)1~1/:' -.;)_ 1.. /;,L) It./_ \0 J_ X C•c' ---:, .... . ,) .) '2,k1i/4< j()/1 I 3 x· l)k-1,bl /J/.(l..J {,,.J7- ."&tf ,.~ 'r 6~ ./ ;!.;>;' -, IJ/t1.Ni_1S20, As - f/l(J!'EPZ11..i-:Pv£ Possible Hazard Identification // Sample Disposal Note: All samples are retained for six weeks from receipt □ Non-Hazard □Flammable □ Skin Irritant/ Q.Poison □ Unknown □ Return to Client 1 i'bisposal by Lab unless other arrangements are made. Tum Around Time FJeqi/ired (Prior lab approvar'roqµ,red for expedited TAT.) QC Requirem__~nts (Specify) LCVP-:~ •? ; •• ; I 11a'Strmdard /{l/"8ush /Spedty) / / / / t. RelinquilitJed by ::[" 'j,-/ ~-·· l~~r-T7r.r-; I. r:,-ceJf~/)'/rd_,/ _,:~,.,, Date Time .f4 , , / Z-/?o~/ .... / ;_{"7 .,,,,~· /,,,t~ ,_.,, .,,:; __ ,. 7~ ' - 2. Rslinq~ish.ecf. by\,, ,;(,, 1 -✓-.,/ _. Date Time -;)( 2. Received by Date Time / -f:::.-"cfl./J( '/J/:.._ _,(,,/~ -;:;::, "?-/ f!',. 0 '5"" /,f's-' , . / 3. Relinquished by Date Time T/s';r/ rec("" b/Jl. G, ( /J ,, Date ;!},me/ /J. 5 7 J. -1,fLJ!- Comments LAB USE ONLY Received on ice (CirclB) Yes No Ice Pack Receipt Temp_ ·c DISTRIBUTION: WHITE & YELLOW-Return to laboratory with Sample(s); PINK-F!s/d/C/Jent Copy - ~ SHFALY ~ Chain of Custody Record Client t: J/,A{ ---f</ fli. jp(; --(-;,,c_/~ Address <Po ~Y S:-o:147 . City s 1,/4 ft. 6J,,J VI 1.-tE [;~ lz;~6fo Project Na~A-J. 7CoNA-PtojectNo:Jli,~s I~ PO. No. Sample ID I Description Date (Containers for each sample may be combined on one line.) . '1>0P-/ l 2}li£ S-J -1 ..J_ ( SHEALY ENVIRON!I/IENT~L SERVICES, INC. 106 Vantage Point Drive L U 0 0 :A If? 0 3 Number 43003 Cayce, South Carolina 29033 Telephone No. (803) 791-9700 Fax No. (803) 791-9111 Report to C~nt~t ,. ~ ,;., ~ "'1l:: "'1!4'-'7 .. Te~No. rgx No. I E-m/J Quote No. f✓ < , -. . ·. ~,..Z,tL· -9 ',,) 9¥9.,1, ~-9~-...a., sazu,e ,£-Waybill No. I Page Pot __ X . p •· Analysis (Attac~ more space is needed.) Printed~ / .. "~ ~~. 7: 14-£/4.,fv /4~(# ~, No. of Containers #, Lot No. Matrix by PreseNative Type UE I ~~ ~ /J~j nme "° ~ i ~ ~ Ii uu I ~ -~ ~ , ~ ~ Remarks I Cooler 1.0. < < , -:x 3 .,. )( sH=' /A'.172ofl.C>c J1tJ:t il X '< ~ ;Ji,;,t;Js1-S- ,~J. 7 X X • ,r-;2 113-S 7 ~ X 'k-1,bc II I ,ft. S ~ {1-3? 1731 1 x· 1x· J}-cJ A>vll JVa. (zd,, ?. EB-tJ/ ~ /?/4/ '3 .... x· TD-3 ~ nL< 1130 l ~ )( -ro-t/. ' , ,.JcJ .,... If ,J(,,I,, I X '\( (f'-J.9 . )34 X: X 7 'f)u?-~ -17 ')( X ' ,,...., ' Possible Hazard Identification □ Ski/4nl□ Poison Sample Disposal Note: All samples are retained for six weeks from receipt □ Non-Hazard zf}:lammable □ Unknown □ Return to Client I' Disposal by Lab . unless other arrangements are made. ·;r Ay~~uired (Prior o/pp7 required for expedited TAT.) f QC Requirements (Specify) Lev a :.zr:. Stan Rush (Specify) ; I~ {,Ashed by 7/j// -l;tl,1.lr o/?)d 7Rec?J:o/ ;0~ ff °!.JI 7 /4.._ Time / 7 -7.' U -' -2.Retinq#~//V/4 ,'/'--l~f¼ 7, 05 1/9.35 2. Received~ Date v Time 3. RelinQllished by Date 1 Time rlls£ sed 'fx_,c; (;,(I._,, 1 ~ate/JO<: l.Iime !~ 1..<J . I. . . Comments LAB USE ONLY Received on ice (Circle) Yes No Ice Pack Receipt Temp. "C TRIB - - WHt-LLO._,tol..., with-(s); P-<VCt; .... -- - ------ -- --Chain of Custody Record C/Jent t· ,/? A Ub l-f;_,?/f t,fSl,rt:/,f'lkf Address n, 7sc1x /0,;ll/7 c;'r,, . -!Al PftJNil/£;{(" ~r· I ;t;2J-a Project Name I C.AJ,4-/ I /C-oV.4 Project No. ,;2 [, 4f'J~ PO. No. Sample ID I Description Date (Containers for each sample may be combined on one line.) I ------------SHEALY ENVIRONMENTAL SERVICES, INC. L o 5 0-~ / 9 O 5 106 Vantage Point Drive N 4 •') Q Q 1 Cayce, South Carolina 29033 um er · ,.) . Telephone No. (803) 791-9700 Fax No. (803) 791-9111 Report to Contact --r-Li .---.,-,,--, 6~ Tefe~e No. I Eax.No. I ~I /~ .. Quote No. flr..,,J...,/;:Jl.K . , .. '&'-(-y/;,J-9 r1/w/-f!t,') ~;1/ / ---y saztu,e ~ff· Waybill No. Page_L ofd_ X ✓,~/~~ ·· Analysis (Attach list if more space is needed.) Printe~~ -' ,. j7Z,p.,tl'/Z'7 I< ~,l)JflVf'l_) • No. of Containers v, Lot No. ~T Matrix by Preservative Type ~· " \'j Time il;?, ~ ~ 2 ~ g 8 -~ 5 :ii § ~ J a 1., ~ ~ ~ f a Remarks I Cooler f.D. < < ~ ~ Jl}/-7·7 r¾·it /,J~ t '· I' ' ~z . /,l}ffc~;zi).: - !Ill-L/R /3,(f ~ o?tt1?-.( . ' J,S C-'/C/ /~v r;:--3'/ lb/1 :f.. Uv v,.nJ ?.it:<ft/ll,'lil fr-b). 4 I 7cr-; • /ft.,f,t,,,,,N,_9S1.tJ1 t~1, --rJ:-,p 'JJL4/lJK -~ :l 1, ·/ -J</:fb ~~ t';;--t, I ~I,,./ / /j /{130, '? 1-3-r-' ! 1:J'-!t) 14A-s1 /433 £1:---5-,f ' Jl(3 ' ,,, . ' Possible Hazard Identification // Sample Disposal Note: All samples are retained for six weeks from receipt □ Non-Hazard □ f;i£1mmable □ Skin lrritctnf ..tJ Poison □Unknown □ Return to Client . / Disposal by Lab 1.mless other arrangements are made. ~ Arou~Zi Required (Prior lab approiia'ruired tor expedited TAT.) , QC Requirements (Specify) iEVn-rr:. pf/ / / Standa /. _ 0'Rush (Specify) _ / / • ,-1, Relin<lfShed by ' I --~ -0~11-/4 T'7'7)D 1 Received"[/ J :-:/ i/ / i:f 1/i '/;: Time /" f,tf?-77 -_, /" ... .,. ,r:( 1 as l7~C "2. Relin/r/'/// #, ~ ~ ' 13/, ',Ji 11'"iq35 2. Received by , Dare I Time 17 < 3. Relim;Jl,1ishecJ by ' Date Time ~ra,o,y ·~ ln c-r: u Date rl'772.D 'I"> A_,, J • •~ ., _17.(),5 Comments LAB ()SE ONLY Received on ice (Circle) Yes No Ice Pack nece1pl Temp. "C DISTRIBUTION: WHITE & YELLOW-Retum to fa_boratory with Sample(sJ: PINK-F1eld/Chent Copy ~ ~y Chain of Custody Record Clientt,.· ,_... ,_,'l,;Jt -,n., ?,t f,f.C{'tJc1.,r7e--.r Address 0 feJj-<fc:,:J $1 ) CUyJ,. I,{,,'? ./4-,,.,f/1-l ,c:-~~· I ".2?uo Project Name.---;- I/ Cct/1/ /J Project No. ;?t,r0.r1.r PO. No. Sample ID I Description Date (Containers for each sample may be combined on one line.) ?e-u-I 2/41 l7, -,:,' 7EZu-3 (y£LJ-i SHEALY ENVIRONMENTA!.. SERVICES, INC. 106 Vantage Point Drive L U!J U li. ~3 03 . Number 43011 Cayce, South Carolina 29033 Telephone No. (803) 791-9700 Fax No. (803) 791-9111 Report to Contact •. Tefe~h_one N9. _I Fax No. l_,,E-ma¼, <> _ . Quote No. ✓€?</lY ,E.,,,z,b J&/. J7?9. -:?'fro /1~·/t,? ~;3:,9 ~2natu,~? Waybill No. / PageL o, L PrinWdN~ •Analysis (Attach list if more space is needed.) ,. C~ai., 'T. ,k I ,vf,t( 1>-r..J ~11~ -~ No. of Containers Lot No. ~f Matrix by Preserv_ative Type ~. ~ ·I ~ y ~~ Time ~8 ~ ! g 8 :-[f 6 ~ ! ~, ~ < •• ~ i' ' ~ ~ Remarks I Cooler I.D. /3£/3 V ,,. X )( X Sa:-") ,,fi-k afl.~c><. i</-0 X l-' X ..,P::_;16,f'JXJ t1t(3 X X K 'ou'?·-'-1 t --p )( ic )< 'TP-t fl Pltfllk. -3 ·2-/2,r o9oo ~le I~ IX :f. ?l6c~t/,ffll £( lw'Jl. A, ;/ct 4,2..J~.tl -r. Possible Hazard Identification □ Skin ,,L, /2 Poison Sample Disposal Note: All samples are retained for six weeks from receipt □ Non•Hazard ~mmable □ Unknown □ Return to Client ~"Disposal by Lab unless other arrangements are made. Tum Aroun~'equired (Prior lab 7,v,Y,}egtJired for expedited TAI) OC Requirements (Specify) .L,6V~-Z.... 'JI-f.J}. Sta.nd,,j;J, Rush (Specify) ;1 / /,,iliishedby Ji~ < OaX,,/4 17:1~ 1. Received½ ... ~h / Date Time 1...--; ..... ,'. z,, 'k ·IS-,.,.. /'hl-,1,-~ ?·;?,?d6 /__y.'? L ,;::~, "'--2.Re/i~ ror.L/J:A-i ' , , Date Time 1uate Time 2. Received by #-f,/,5 /'?tPS 3. Refi~uished by Date Time 3. Laboratory receiveh? /} Date Time JJoS--T1.s11 S' L, C, C,M If. J, !{,_ oS Commems LAB USE ONLY Received on ice (Circle) Yes No Ice Pack Receipt Temp. "C ... IBUW.,,HIT,...LOW-tola~th,_,);P/,...Clie--- --- ---- I I I I I I I I I I I I I I I I I I I Purged Well Sampling Log Project No. Kubal-Furr & Associates -E,rviro11111c11t11l Co11s11/tn11l1-Sile Location CNA Holdings/Ticona, Shelby, NC Field Personnel G-1!.. I '3 5 Well/ Sample ID Weather Condition v:v4l SwM, Semple Dale 2 / f s-/ c,~ Arrivol Time II 2Lf Sample Time_--t-.-'-'~-+---- Descriplion of Measuringl,...,.,r 6l,,' I c . 1 @J.s L k' c [2J Casing~ Po·,nt (l,'P) i" os1ng ype oc. 1ng op V 0. 1 1 v 1ome er ir.ch"?s Total Depth of Well Below! L/ L/. ~ Q I t,,IP?_ l~•~t Common Gallons oer Foot Conversions ::=====::::::: Depth lo Waler Below ~IP?I 3 ')5, 95' ,.J ::=====:::::::::: Colur:,n of \Noter in Well'?( i O : q 5-k·ell ::===::::::::=:::::::::: Gallons oi Wol~r per f..,o:I {J, IG3 a 0,110°" [see chart)? Go!/ons of Water in Well? L ,g cell Gallons of Waler to be 5, 3if. J Purged i3X)? Purge Method? 6 Cli{(/ I Purge Storr Tin;e/ t 3i i I Initial 1 1/4 in Well Casing= 0.064 gal/ foot 1 1/z in \Nell Cosing = 0.092 gal/ loot 2 in Well Cosing= 0.!63 gal/ foot 3 in We/I Cosing= G.367 gal/ toot 3 1/:_ in Well Casing= 0.500 gal/ fool 4 in If/ell Cosing= 0.653 gal/ foo: 6 in Well Cosing= 1.469 gal/ foot Total G0l!ons Purged/ 1) goll Purge Stop Time( I 33·2 I . 2 3 4 5 Samples Collected Container De5crip!ion Preservative @-1,v>-,___ c~ y-1:rL2i i'l:,~4 !G.42- Remarks ________________________________ _ Parameler Conditions: pH Turbidity +/·0.1 standard unit +/-!0% above 10 NTU COND/Temp +/. 3% +/· I NTU below 10 NIU DO ORP +/-1 G% +/-!OmV. .. Revise 5/28/02 Kub JI-Furr & Associ.1tes P,x:;-o: 1:-,·:--.,:c': {-ie (x"'~fl'.j ;,,~r.;,= ~~-:::-: 7·,-.1~: // :S: 1;2. ·,,:cter-Level 1\\eoiuremenf5 : .. ~ 11 " (,I.) iJ : 5 " 17 13 " 20 I I S-:;rr-ples Coile<;; ttld t/4%, 9 IO II " 13 " 15 16 17 ,a 19 20 --- 7 7, I 7, Field Poromer:;;rs c--~. -·~--..:. i.·~~-·c:-::i t.',TL'I [:,;;:;· • .,i,: 0,·,-;::a,-. (mg1~J ·- Cor.t::iiner De;c1:::.:::::., g '< tf.0.i t It~~. " z:s'lh. ------.u~ . .,.,,, -;, ) .· .· 7" I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I l::i'-"•,=iow ,:;,,:.u~c .-:: :::: Sc.-n~:i,-.g !.::lg Pcoject t:o. _ __,,J_(c,_, 6__,,_e_jl_--J_ Kub.11-Furr & Assod,ltcs -£1;:·in>11nt,·n.'<1! (p11_,1d.',111/;;- 5 10 II " 13 16 17 13 " :-o ,.,.,, ... ., •. ;,, p,.,..., Y.,.I\ •'-S Pu;e S•a•, T,e•e;J.!:f.1___7___ ' c, i /l: t/1 _, ' 5 I /7, 't 10 II : s 17 i·-i ! i 7,'-f'j, / 7 7"l i j /7 ?C:..-I Con,01ner De,c:r,p,,cr, field Porcime:e-rs --,- ii i (c 4.'fl 11. 7 / c; i 1.J. 9l O l I c,:: O,;'g~:-. (r:",g/Li c:; 2. (, i I <;<;, 3 c; 11 I <J7. i • C:P./Ti~ono lo·.v-f!01•.G:ovodwci!er s~"';:i:;:1g L::ig Kub,11-Furr & .--\ssocijtes -£1:;•i,-,,11'1:c•:1:,:: Cc>ll,C/l/;,111.'_; - Pv-;~ ·.•-:·.· .. :,1'. ~-C:?'/2/"?<.. P·";• s·o,, ,.,.,;7s=9s Vioter-Levei ,'.teasurements -~-,.ec·•.~ -----· • D;-.,., (:ee:; l" ., 0 i ' r) i /cJ)' i ,. I I, .5' ' iat?</ I • ' I ' i lo ' 12 -::5 ! _.J• ' 3 ' /.j I 77,,=<-J ' I J.o ; /47,:, ., 5 ! 1s· I r~ir-j 6 I ' '..)o I /(;.ID 6 7 I '.3 ~ 1. /(,_i"o • I ' i i./ 6 ! 17,IS ' ' I 'is-' i I 7,7G 9 I 10 I 5o I /x)c i-) Ii I _,-s i '; J.,r; ( " I 12 i &ic) I /9.o( " 13 I [,.,;" 1/9 . ..ro I} " ! 70 I ;1.,fo I' 15 ' '7s I ! 1-t,;J/ IS 16 ! I IS 17 ! ! 17 IS I I 13 19 I I 19 2() I I 20 " ~<..:r ;;e 5:.J,:. i,r-·-: '_LJ_Q_Q_____ Fie-i-:.::: ~cr:imete:; : ' --! J/J, J,, ' &{., GI.fl, '11. fcJ I , I S:tl• · kL~ 9-'Ju I t},(1N I., -1 1_, ,O-.J I {;; · 7-.1--s-1 Io,:, i 1t/.Jr-: (,,.1 '1, 1t ! 'I /'f, 7t( ! !,;6 '7cc i / j ; iL/ id ; t,G I. II i /,;}, : il/, 7(, \ (,·{,_. r ?~ , . ) i o. 'l IL/,7f &l.-.. '5/, ~) i • I U',. : i,l'O : I 'I.if i C,G f,9, i /3 /'id2 ' L,y;-{i 7 ! ·' ' • I '' ,, i IL/, f.r: &q 9 :3c, I ' '7 I , . i l'{J,7; lv °t, ').f 'L{ ! I lt.i.SS : (.;-;; 9 ·r'IJ... 0,9 ! i'{,,ff.! L, J c;_ 'Su /,o i<t . .fr i l·-) <?, ;'./.(. /, t./ i I I i ' I I I I ! I i . -' ; '1£/J ' lsf.'1 i /,'f(< l/77./ . 1,/,k il.f<f.1 I 0, C,'<( 1/99,9 . /,6/ I 2, 3. '1 I!? ! ');,(,'/ • I, I 3 I a12s I ,J-1 I, l'1/,J i ,fJ I /7/ [., I, 'i <( ! /(;z ' - J.,f/ ! /,t:3 . , :;!.,di• 1/.~;J,, ' J,J.l I 1cs✓1. -g_ i 2 3/ I ; ~o . .J, :2, -:Jl / I S-1 I ' I ' I ' I ' i I •. ' I . ' I I I I I I I I I I I I I I I I e,mc,,, ' /~17AC fi-/ZIT.A..2b. rv1,p,,vG' .H .Jlo•v .1S ?,rJ,?4!, 1/,-1·r,,•;,c,;l7 }Aw~,,-,, ;),ca· N•-r j'TM1'12,: -.+tL ,,,11\.-" j)M;/,1,e:JI«/ -s;:,t;\.c· -u ... z. ;1 .;i'> -r~, .J,,~~,~~-·-,,.f: ... S4.•._;;i ft"':.!~·t:~-~-~{: ·rl.} ,, . .,.-.1.':.:-t1~~1~:17,t11J I ~.;-";;,,::; __ , ,...-.. ,._,_,,._. __ ,_,..,,1.. ____ ,,J/1; -,-__ , l,_,-,.,._,, T:.::::::~i:y •!-10% c":::i·:-~ 10 i'HU •/-I ,'HU t.a:: ,•; 1-:. ::i1_, o=::: -:. ](,--;-,'/ I C:!>,/fr:o-i.: Lo·...,.fjzy,~G,o·;:,d.--o'd' i::-rc·i,,c Log I I I I I I I I I I I I I I I I I I I Low-Flov,· Grcundwo;er Sampling Log Kub,1l-Furr & Associates Pro_iect No. -Ei:,·it("1111i•11tnl Cu11:-1dt,111t::'-Site L:Jcot,'on _C=Nc:A,_./Te,iC:.,Oe_nc,ac:•..:S:,.:hece,olb'.Ly,_, ,_,N_,,Cc...... Field F'erscnne/ _G=,-'.;..(L~· 1-/"'/,'-"'-::,'~----- Well I Semple 10 -'--r=.,_F_'_-~3c...i..L/ _____ _ Scmf.":i':! Jere 2 1· f )/(J S-r.:rscl Time I. <::,1;.5lher Condition _",2. 'J<vcr:Y>cc'-::::-+----"Lc,' ~c.l'.::'·:...'...:':.sC>c...'->::.' _ -l L--.J. Semple :"irr.e f Z.. -,. :;e;,::•;c;1cn of ~,ieo!uri.~.g: f ((){___ i Cosin T• e! S lxl:ing Ccp!i l-/ i Ccsir; 2 I ?01nt IM?)i : g IP l S', 1 Dicrr.e;,:, r.:M" Pi.;rge Met~cci e~~-,·skl h 0 Sampling Melriod!'=('e_==i/=~=:1:=<-=--.r=~c-."-'-,-·----"'"" ?~rge St-:irt Time; I 5yr-I Purge !·.::p iime! f (_, j '-\ 1Nater-Level Measurements Field Parameters 0 I l 3 ' 5 6 7 8 9 10 II " 13 I' IS 16 17 18 19 20 i I i I I Elc;::.,se T1r.,e (m,ns) 0 < /D ,s 2.iJ 17~ I ~"'_, i --Z..,C: i i ' I I i I ! I ' I ON/ lfee:) I /(!,OZ- i / D. ;:, 'K I /1) <?'i I /0.'iu I /l! c17 i in. 'i'l i /(J,·]2. i in. 'i 1 I. I i ' I i ' I I I I ' I I I I I I I Samples Collected Rerm::r~s , :J l v 0 I 2 3 ' 5 6 7 8 9 10 II 12 13 " IS 16 17 18 19 20 I ---· i I l'J,l.'-{ I i i '7 I I i I I IS. r,9 i I 1"i 1,li I \ "7 " I . I·,() I l;c:..1-1 I I Ii,; 0c, I ! I I I I I I I I I I I I I I I I I I I I ' I I I I I I I 5~ac1fic Con,:l'JC:once (;.;Siem) -· ~ '.>{ ),, <, (;1 1l: Y' )(,• ~(. '2,C., Container Descnptton i -I ' f,Jrbic,:•; (~-!TU) -- I -~·-I ';),.) ·-. I '5.li') I '?. I I C, c.,c, 14, 2 I I S/'ii 17 .., ' ' --, !",,<:.;7 I 7, I ' I c:; . .:;Li I I 1 I ":i S'L I ri 1,<. ' ! i I I I i I I I : I I I ' I I I • I I I . I Preservat1·1'° :)isscl·1e:: o~·,.ge"' (rr.g/') . --I -' 4. 'i'i: i I 2/ <;- 7,,i.,7-i / zz., 7 Z,~c/ l/24,<, 7,G'if ! 12 /.:. I l, 5D l;z1.,g z...<j0 Ii ZC,,G 'J. 7,;-! IL/, 7 I I ' I i I I ! I I i I ' I i. I .. • pH +/-C. l st~ndord uni: CQ~:O/Temp +/-3f, +/-I NTU below 10 N:U DO -i-lOf. rurbidily +.t-10%cbove 10tJ71J ORP -:-IC~n.V .. CNA/T;cona Low-flowGro"!ndwoter Samp6ng Cog Kub.11-Furr & . .\ssodates -£11:•irt>i:1,:~1:'.,;; (,,lli///:.:11.'~ - :cccele Coe, ?_ I IC ( c\ s Oeso,,,,:n:'':'="-',·-.. ,.-r,OL •,·. ,:,,;g;c:.',. ,, i. -,1· :-~,r.t[.'.';,J; Jt.: ~ ===--------?:.,~.;;-= _•;~·:-cc -t,1.:... ... --:s{-. .../ .J.-.L. S.::.~::•· .. ~g ':'="·-:-::. t'C-../< .. -'~ ~L·w ?cc,,:,,,,;,,,: {J-/ £."/ : "v'/oter-Level /1.i\emurements 0 2 '1 0 , I I i ! 17 7<; i/7 '-1-2 Field ?ara.";".eters 0 i _ ____. ! i --- 1--- ,_ I ,_ ' -I - i -- "l <; ' 17 S7 5 i 15, Zi{ ir';L/ ' in. l 2 I ~ 15" 1, 70 i 1'7 0 15 " 17 17 18 " 19 20 20 Cor,:c:.1er De,c11ptiol'I Pcrame:er Cond::icn,: I I I I I 11 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I Kubal-Furr & Associ.1te5 -E1::·i:·t1•1111,·1: .;i Con;:1!:.;:::., - wo,-:;r-Leve: f',,\eoiurernents C ! 0 :~1.t.ff I i -) i~.'.727 -' I i) '3"2 j.) . I ! /s 31,</o ' i Jo 3 Z. </'{ J~ 51 '-IS' 0 5o 32.</l ' ·S s-JJ. '( (, ' ' 1-:i Ii I' 13 I ! i.! I 15 I i ' " i I ' 17 I i 13 I I ' " I ! 20 I I Somp•-:?s Co,lected ltz:( LC•N-~·::;•,v :::,.,2,,_, ... ,c·.~·::;~~ 5,::.,.,..c;::ir,g Le,; Frcfecccro. ~~-l--iQ_JI_~_ 0 I ' ' ' , ' , ' ; \(' Ii " I l I' ;5 " 17 13 II 1() Field Pcrameicrs. i -r ,_ ! Jlf/i3 1 -;}Ob , LJ. 90 // I /7, f7, ,.f).L{ i i Cor.to,ne: De,cnpt:cri 4,93, S,'J (/.9/ I t./,(1 '-i.. 9 I ,, t./,c> -1·- 0,2 .• -, 217, 'I er J.3 i ;l1'r. o Cr:>/Ticor.c lo·,•,.f:owGro~•-~~,.of,;,r Sor,-;;inQ Log Kub,1!-Furr & Associ,1t~s -£.•1;•iic•1: ":,••::,;! C1•l!::'/l/t,11:!~ - 0 0 137,/o ' : lo i -3'7,;Js' 1S' 37,tff Jt, \ 3 7,Jv 8 10 Ii " 13 15 16 17 18 " 20 QDl.1 0 ' J Ii I j :.: 17 i 5 i- I IS,?;/, /.{,'/3 //.,, 91 ! / l, 7.s' l I i I Container Descri;:'.,on Fie.,J Parameters -!---1- i./9 I l,, )Ji .:37 I l,,JJ( I "31 ! G :;z.9 i 13 ! /;,, 3 ~ I . / 0 l,,331 9o ·-j- I, 3o I /77,J I -, -10;;, C~:> -.'-IOmV I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I Kub.ii-Furr & .-\ssoci.ite5 -En:·:•·,,,:11:,·n:,1:' L,,1:-:1:i.-.;,::f -CNA/Ticona · Shelby, NC cc,·,~g·, C:·ic:"'a'.7r. ?v:;;::: ·,:➔,:-:c, f ,:.> c"-; ..J:cJ J ( ,.-5.:;,":"::•i:",,;; ,•.:2··:.:: /:e,• &,•"SL, J; (.(,. ... 0 f C J II i:? i5 16 17 " ,,_,,,;,cc·;,., /i)-S: 'ac;frcc:.~, ~; ?cc;e'oc,'. 2._CO __ , __ , c) :il,Jo G ' /O 7D iJ,1i"! ! L\C 17. 7') I l 15 ,, 17 " :o Field ? .::r0me \ ers I ------! ' --i -i \ i i ' "i'i i 111,.71. ' DO +/-I:,'., O'=:? +/-10rn'.' \ \ \ er:,;/Ti~-:cr.:: l ::,·, .• ;:•;::•.~Gro•Jr,dwoicr S-:,rc,1'1;; '.:; Kubat-Furr t.~ _.\.55;Jd.1t~s ~E r:·it,,11m,":.•.r:" ·:.":.':,.':.:· C :;;_ L/ ks • 1,-; 7', ·2.C.3·-} ·?.( _cic\ ?."\ ?7 ~\; ell_ F·,/ -' . >/,Cic I [_/ (· : 2 .. '"i '~l : )c· ,,:;i:_) ?C' ((· II • -;; I ,CL " I )/,//,., 13 I -7_1 ,-' : '!-) " ! 7 t_, I :,i.YS' i i 7~ ; ::/, 7 Li 1: I i (-, SJ ! n , -, 7 )::. l. I' '1 ,;·:;-i '?, l. 52. 13 i j i I I i 0 I ' 3 ' - ' 7 s 9 IC II " 13 " ; :; " " 15 " 20 ' Is-· n 47 I Lf7 J 117u , /4.GS , 41() i I S, 7:? I '-ti({) 1 i l.:.l'4 ! Li«( r,_:t::::·. (><C•_'J 1-- , /_,_:_/ 7 i / 3 , (. '-!7 i i" I ,,,i i (. ',( C;,·1~~17 i,TgfLI l .... -1; ! C 0, 7q (), (I (J;I 7 . (} 17 027 /'j L-: Zt 0, 2_7 -4 <~/, ·-; -)-Z1 I ' --4-'7, 1 !-~j) G 1-/J --,1 : r ) , i -L/{ ,[) i -iJ~-7 ' , 'i -<~s· 1Y I I I I I I I I I I I I· I I I I .":,ee:-c:<,; i->~ j()l!i .-frf-i... llJ[,~~;i_:..,, .. , ... tc"\-t:,'~ Jui-:,; :1 ,2c\ J•\-' 1)/;J t-.,·l .. l( -n .. ,L"-T"t,· j1H/t.J.-JiJ1•1(,, {lit-" r'c.---iJ),.,t-s.i:(:;;)) -·h:f ,'l /1L; rp,t) NI t::\.t;~L-, _"J • .:.; rr, i:i)-J ()t.sr "/l• .<a,-:i.--; <-'01,.i✓.flpv/rt' ~ .. -,Zr}·£. 111,.-· 4., •\)j•L I L-H l)c·,-)i,(;,., J,•f _,\\ ;r.t:f:-t:, ~<-i\ 1 'ih.'c·1t ,Jft· ;.1,-,;,.f': 7j tJ :.if. ;11v.•r·~77p)ti -l[1l ,1TJ/J..:.:L /r:.-t-t~'7l" ·z_~ s·i:::1 .. :·L ,,.._ }Jc:·c,1:t•i) rr-J_·.·;-..,.;,1 .... -. Pa'.crn~:~r Cor.d:1icn/ ;:fr'. +/. o. /s1onct::•j un;1 co,-:or;~mp +/· 3~ 00 -/-iOh i•_::::;::;:1 .. ;. 10% a':.:'.ov~ 10 ~liU +/-1 ~nu c;:;!8w lC' / ,!;J o.,? -/-1Ornl/ I I I I I I I I I I I I I I I I I I I I Kubal~Furr & Associates -f.11:·i:-:nn:c·n!,1/ Ccm5uft:111ts- GCJ!lon, of 'doter to be Purged (J:<)? ;8;./,L[>t... I Pur;J-: S~::irr Time LI _ _,(~ . .J.'--;_,C)c.._:L /_,•L=_· __ Common Ga,'lqn5 oer Foot ron'1er,iqn5 I 1/;. in 11/sil Cosing= O.C:'2: goi / foot 2 in \'/eL! Cos:r.g = C·. l :;3 g:il / foot Jin '.'le!: Cosir,,~ = C-.367 g.::I / f,Jo; 6 in Wei: Ccsina = 1 . ..'.:i? col/ klot To!,:il G.::llom Purg;:dl ~~,-,.S-c~ I Pccge 5:op Timei r1'f 72 Initial Voiu,T1e Purgec I 0 cai 2 1,S-J J 3 5 - eel c:::: Jf T 77,~e i:;," .. .r/n Jl i,1~- Time Ternpercture SpecHic Conductance pH DO Turbilidy ORP c--912 If:. 7::c 1(',h,,J t I 7 ,, r. /,1"{"'" O,'i /2,:,,'~ :;z I 11:u -l(u,> m, s9:-np!es Collected -- (); .. -i/r:;7)/J-vt· -t C{~ o:;22 iy,(,;"/),c 'C /)~ (,)o..,,3 V° j "' ,;/ )/ (, 0,/ S)l I ,r;:;;L,. 1 ;·d unil; ;:j ·-·~i:; • '.fa ' /' /, l~n/L IT'.';,'<. r.c·c/L ~6wu · . .-/ / 1:11: ~:L' ·-JZ&J mv , / r.,',' r:-.'/ Container D£!iCrip/icn /'r..7.~Vh I ],_ )('fl':•i . l / 43 ~5 /'?, 0 20S-4 S;21 / :..l. ''''"J ~°"' !lil' r,-',' ·- .. Jtj .... ~::; ,.,.._,.. '. :,7J ~:: Preservcti·,·e ;fer / ,o3 -, i I .":> 7 -/3/} -Z,J. C A.-{;c1;/ &~ Rer:1c(-:i ________________________________ _ -----------------~li='--=J,c.,"=-z'c''l-f), k&c,(} · 7 U,o '"'1J/L Pcrometer Conditiom: pH Turbidity +/-0.1 standard unit +/-10':ocbove lONiU COND/Ternp ..-J. 3;; +/-! NTU bel()w 10 ,,:ru DO O,? +/-10~ +/-IOml/ Re·,irn 5/2'3/02 Kub.ii-Furr & .-\ssoci.ites -£11:·i:-(•irin,•11~.1/ C(PJ1~11i~a:::_, -CN~/Ticona -Shelby. NC . . . .=·'=:.'c P=rsonr.:1 ,:--.,. '-1, :-1. ., ::-:,. ,'. •• _ .. C :=;::~c~1or. ol -~;~~~.'.'.~~: 1(:,j [.. -~-,~: T .. ~,.! :') L~\ :=====-~___'-----'---'- P<.;rgP> ,'.',a!.~.:u1 /\:;.\' ;\-·.:_i 0 3 3 10 12 13 " 15 17 13 I? ?,.•r;,. S:r:::r: i1n:e: 0:-;--:;-;- I E'U":cB f1r:'➔ i~-ir-.;,< Samples Coll,.,.::ec C 3 l7 ?J ?·Jrg➔ S:.)O 7,r:-:➔ _!(10i.J -.-'-~·~•=1- T-:ir:·,:::a~-::: .r➔ 1'.::J field Pcr.:irneters :: ••;,;➔'1 (;":".glll I -------! -·----·-· ., I ·,j 1-c 'iA )i)'j L--, 7(1 ! ~.;, S /7, i,'l C, 7S , 1.i, ; 1\ ,J (;-, ?(. 1 U [' (; jL . CO~iD/T€lmp -r/-J;'; +/-I ~,ru b~'.O·,•,' 10 tlilJ D:J -/-10% 0~? -/. \OmV i -/A-t, '2.. I i -~i,{,_;, ')_ -(:),/,, 3 CNA/Ticcr:~ low-FJo,.,Grou.'\Cl.,,c!et S;:irr,pling I.:,;: I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I KubJ!-Fua & .-\sso<:iJt1!5 -En:•fr:;11,•:,•.,::.,c Ct"!;:,!:.:.•1:.-- 0 ' 3 ?,.•;~ _.._~~:-,.::-~· (--~,.-<~-t:.../-hc.:,.; .,,,,,, :::,,-; [c,,' i 1-4 2(,, 0 0 !.:5::.-,·,; r--'---'-+-"==-''+-"'--'-"-±+----;.-c~+-½,.,..----,u-""---'-:,,:.-'-'~--=,:....c.--¥'-'---''--'---'"'-'-",...\ I f--'-~..i...,-'--'-"'"--"'4-f----'--1'--"'-.L!..-'-~~--'--~=-k-=l:---~'--',.-!._!~.J.J.:.:_Lj 2. 10 II 13 1---' '---'--l-'L---'--'-'-'-""4------'-..Lc"-L-'-"-'---..L-'-''--'-_J.""-'"--'--'--'=:.........:J,..==-!.==e::.i I I 5 I " I I 1-. , - 20 I I • I 1~ II, 5' - Samples Col.ectej Can:::·n~r O~scrip;ion C~lA/1:cor.:i Low-flo.,.,G,our.dwoter S:i"'p~rig lc;;i KubJ!-Furr& AssociJtes -E•::•ir('l!lll,•11:,;i C,•1:~1::.',;11.•~ - "'('' -; . l'A -L1;' ·{JI 'S _ 2Co ·, 1-/"J CNA/licona . Shelby. NC I I I P"' ,1, ~--lr.<-s ?•.r;-: s:c-~ ;:~-? j ,.(3G:.· Water-Leve/ t\\ea5urernenl5 10 II " 13 I; 17 " Fi:=id Parameters 10 II I' IJ 15 16 17 18 19 ,0 Con!oiner Des.:ript.01 ?~r;; ~=·~l Do ..... .-,.,..). Ci~10,·,;~ 0,-,.,;-:l·-c,;:;, 1~-•;1 [n:g/~i - ·1 .+1 i_ll.1.0 2 t.f," i-2.2 ' ,. I I I I I I I I I I I I R;""::,<s __________________________________ _ I c,H +/-0.1 s~ond..;r:: u:,i: ;,._r:;,<oi:.,. •/-!0% above 10 r:;u cc,:-::;_,:s:n;:i ,1-3r, ~r 1 tlT'w' C:-:ow 1:j ,'H'J I C,'IA/T,ccr:;, Lo·.,-.':owGro~·:-,d·.~'O!er $:;,:11plir:,;, L::,;, ' I I I I I I I I I I I I I I I I I I I I Samolino Loo-Grab Water Samoles Project No. 26QS 1 s --'-~--- Sam p I e Date --!-:)1/_:_'J-.e.}-1--/2-=-t:_.l __ '7Dv-r Sample ID Site Location GI.~ I Ticona -Shelby. NC Arrival Time Duplicate No. _l)~v___,_?_-_{,.__ Sample Time ~[_'s_{~3 ___ _ (-/:_ Field Personnel ------- Weather Conditions .JL'Jv-c~; {:,cf Sampling Method I 1 /J: )/--7 Sample Temp. (°C) -"-· __ 'j___,_-'--(_Spec. Conductivity(11S/cm) Ye pH_'S:_1_9~(- I ')!' . .--- OPP (mV) I ,7'--, ~ Turbidity (NTU) _ _,.:2-'--+1-· _ ___,DO(mgll) _2_, 0_,(,--_· __ Remarks Container Description _$,-\{(,:).Lt I Preservative J/ Cf /l.-~7 J.O· LCT j?..,·.,;p ,2...,v /ct_ f\P;Jl2t-)':. 1 / /.,/1,-•J 'i;;f::,.r: .J)!,,tf J...wt---rco,:;. ·o ')L, (,,, Tl!~ OuPJ ·,c:.o;L-irer,,1c·')/l Pu1~1,)<j f;tu.,1 Cc;'-~-,",,("/ ik '2cv,1·~,') ') I, ')'J / _,----s amp1e Date ---+-/<_11-'-1-./-"-'tJ:___ Arrival Time Sampl~ Time _/--'-(~{'J __ Sample ID flJ-u-L{ Duplicate No. ______ _ Field Personnel ---=~:..;Ic':...;::, __ _ Weather Conditions .su,i1,.,-; Go1 I Sampling Method Sample Temp. (°C) 1/}3 Spec. Conductivity(µS/cm) s-&-l ~ cS: 0:--pH __ .J=-'-''---'U=--- ORP (mV) Meth d(s) ) _'.{, Remarks S 6, I Turbidity (NTU) //} ,"),_'5 <' ---,,'---'-p\_,__ ___ _.cD0(mg/L) _JC."-'--'--_,_, __ _ Container Description 3;('/t',1 Preservative !fc 4 /1/,,:' ,;.,-;ef'&/' f -., l1 29 'li);;-•' d)' C/ ( 0 G:,J~ Lt:T ?'-'••1' f.Y-J ;b"f Pr</:, /frV ~I/;_( ?tfi:1-e:S.4,J,fl L{ Tc<•1<-'1<jtl,.f->?•t"11LlE1/i),/£J' /,uC't' ~ Do /l•i~ 1c-<1.L-<--Af/J) I(ubal-Furr & Associates Revised 7 /30/02 Somolinc1 Log-Grob Water Som oles I I Project No. 26QS15 Site Location CNA / Ticona • Shelbv. i'IC Sample Date __ 2.,_(_~l'-1/4""--=S;........ __ Sample ID Arrival Time Duplicate No. ______ _ / t/3 ( Sample Time_/'_/ 6'.....,,___j -I Field Personnel ___ 0_7<-_'_· __ _ Weather Conditions S~;_.,.,<.-'7 {c,. Sampling Method Sample Temp. (°C) :;J.. / ,J'3 Spec. Conductiv·,ty(pS/cm) L{ 7 pH __ &_·._(_,,_·[;_• ___ • I ORP (m\/) Methocl(s) i.tX:5 s L,cC .r Remarks ~'T.;i;L/ e f v ':J.(,,s --:i_ Turbidity (i'!TU) __ ! i(...._· __ ____:DO(mg/L) _'-'---/_3_~ __ 1 Container Description .'.S(t 0),~l/ I k.:?,cf7S I -----------1 I Sample Date _______ _ Sample ID Dupl'lcate No. ______ _ SampleTime _______ 1 Field Personnel ______ _ Arrival Time Weather Conditions Sampling Method I Sample Temp. (°C) -----Spec. Conductivity(pS/cm) pH _______ I ' ORP (mV) Turbidity (NTU) __c _______ ,DO(mg/L) ______ _ Method(s) I -------~---1 Container Description Preservative Remarks Kubal-Furr & Associates I I Revised 7 /30/021 I I I I I I I I I I I I I I I I I I I Kub.ii-Furr & Assod.ites -£11:•/r,>1:":~11 '.,7/ Ll'IIC-11(;,;:1:_; - Water-Level ,\.1emurements Field Parameters 0 ' 3 Ii " 13 17 ,a 19 20 E:':::~;e rr.ie C-~-·-i~e.:-,·: (e:1:~;J ; /<;" i //. 0(' 0 ' p I J 15 17 13 19 2') : :;-,-,:;• •. :: J:",Ci: 1-.:S:cm) -:-i i / ,0&f · '3.f(, (/ i ,,:; '. ;-:r ::;::-~- (:-:-;-'I -•! ! --!- l/. !O • 8-,f ;• (.I 9 e i 't. 7 c/.'tL! 73 i O,/'S"' i ?-7. 7 c~:r.11:~::";; low•!'!ov,Gro..,nd~.'CJlerSomptln:-;i L::,; I I I I I I I I I I I I I I I I I I I DATA ASSESSMENT SUMMARY CHECKLIST AND REPORT-LEVEL II Client ID: Project Number: Project Description: Ticona, Shelby, NC 26RP21 02/05 Sample Delivery Group (SDG) Description: Prepared By: Robert DeGaetano Date: 07/12/05 Two aqueous samples and a field duplicate were collected by Kubal-Furr & Associates and submitted to Davis & Floyd of Greenwood, SC for total organic carbon analysis. The D&F login numbers were L050504 l O and L05050602. CONTENTS LEVEL COMMENTS II Sample Results ✓ Data are considered Class A Chain(s) of Custody (COCs) ✓ Satisfactory Master Tracking List ✓ Satisfactory Method Conformance Summary ✓ Satisfactory Batch Quality Control Report ✓ Satisfactory Trip/Field/Equipment Blank Report ✓ Satisfactory Field Notes/Logbook ✓ Not reviewed Discussion: Samples were analyzed within hold time requirements and results were consistent with historical data. Class A = quantitative Class B = qualitative Class C = unuseable Kubal-Furr & Associates I I I I I I I I I I I I I I I I I I Df\YIS FLfilD June 15, 2005 RICHARD RAMIREZ CELANESE 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Report ID : AC1629 Page 1 of 13 LABORATORY ANALYSIS REPORT Login Number Project Number Description :L05050410, L05050602 :61621.01 :TASK ORDER #26QS16 -TICONA SHELBY PLANT Dear Richard Ramirez: We are pleased to provide the enclosed analytical results for the samples received by Davis & Floyd, Inc. on May 04, 2005 through May 06, 2005. A formal Quality Assurance/Quality Control program is maintained by Davis & Floyd, which is designed to meet or exceed the EPA, NELAC or other appropriate regulatory requirements. All analytical analyses for this project met QA/QC criteria and the results are within the 99 % confidence interval for each method unless otherwise stated in the footnotes. This report is to be reproduced only in full. Feel free to contact our Client Services Representative at (864) 229-4413 if further explanation of the analysis is required. Unless other arrangements have been made, samples will be disposed of or returned 14 days from the cfate of the report. We appreciate the opportunity to provide services to your firm. Sincerely, DAV'?ZZ~C~.VT,,IJ---t'f-- ohn H. McCord, Jr. Laboratory Manager I Davis & Floyd, Inc. ) PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229•4413 I Fax (864) 229-7119 Di\YIS FLfilD LABORATORY ANALYSIS REPORT Sample ID LOSOSOU0-01 Wot Chemistry SW846 9060 L0S0S0U0-02 Wot Chemistry SWB46 9060 L05050602-0l Wot Chemistry SW846 9060 Client Contact CB'LANBSB 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Richard Ramirez Master Sample Tracking List Client ID DUP-2 V-23 NC Certification Number: 25 Project Number: 61621.01 Report Date Page 2 of 13 Date Collected 05/04/2005 0000 June 15, 2005 Report ID: AC1629 Date Received 05/13/2005 0819 05/13/2005 0923 05/18/2005 1630 I I II I I I I I I I I I I I I I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst ,\venue I Greenwood, SC 29649 I (864) 229-44-U I Fax (flfi4) 229-7119 I I I I I I I I I I I I I I I I I I I Di\VIS FLOYD LABORATORY ANALYSIS REPORT Client Contact CELANESE 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Richard Ramirez Client ID: K-28 Parameter Wet Chemistry SW846 9060 Matrix ORGANIC CARBON, TOTAL GW/Chemw Result Qual 52.7 NC Certification Number: 25 Project Number: 61621.01 Report Date June 15, 2005 Page 3 of 13 Report ID: AC1629 Sample ID LOSOS0410-01 Date Collected: 05/04/2005 0952 Date Received 05/04/2005 RDL units Analyst Date Time l.O mg/1 CDC 05/13/2005 0819 I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-4413 I Fax (864) 229-7119 DAYIS FLiJYD LABORATORY ANALYSIS REPORT Client Contact CELANESE 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Richard Ramirez Client ID: DUP-2 Parameter Wet Chemistry SW846 9060 Matrix ORGANIC CARBON, TOTAL GW/ChemW Result Qual 50.1 NC Cenijication Number: 25 Project Number: 61621.01 Report Date June 15, 2005 Page 4 of 13 Report ID: AC1629 Sample ID L05050410-02 Date Collected: Date Received 05/04/2005 RDL Units Analyst Date Time 1.0 mg/1 CDC 05/13/2005 0923 Duvis & Floyd, Inc. I PO Dr;iwer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 ! (864) 229-4413 I Fax (864) 229-7119 I I I II I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I DAYIS FLtfYD LABORATORY ANALYSIS REPORT Client Contact CELANESE 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 2B152 Richard Ramirez Client ID: V-23 Para.meter Wet Chemistry SW846 9060 Matrix ORGANIC CARBON, TOTAL : GW/Chemw Result Qual 8900 NC Certification Number: 25 Project Number: 61621.01 Report Date June 15, 2005 Page 5 of 13 Report ID: AC1629 Sample ID L05050602-0l Date Collected: 05/04/2005 0000 Date Received 05/06/2005 RDL Units Analyst Date Time 200 mg/1 CDC 05/18/2005 1630 I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-4413 I Fax (864) 229-7119 D~IS FLOYD Client LABORATORY ANALYSIS REPORT CELANESE 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 NC Cenijication Number: 25 Project Number: 61621.01 Contact Richard Ramirez Report Date Page 6 of 13 June 15, 2005 Report ID: AC1629 QC Summary Data I I I I I I I I I I 11 I I I I I I I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I HJ 6 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-441 J I Fax (864) 229-7119 I I I I I I I I I I I I I I I I I I I DAYIS FLtrYD LABORATORY ANALYSIS REPORT Sample ID L05050410-01 L05050410-02 MB41176:l LCS41176:l Client Contact CELANESE 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Richard Ramirez NC Certification Number: 25 Project Number: 61621.01 Report Date Page 7 of 13 June 15, 2005 Report ID: AC1629 QC Batch Report -Batch Sample List WorkGroup WG41176 Matrix GW/Chemw Description: TOC Prep Method Analtyical Method: SW846 9060 PREP ANALYTICAL Client ID •=• Date Time Date Time Analyst K-28 1 05/13/2005 0819 CDC DUP-2 1 05/13/2005 0923 CDC Method Blank 1 05/13/2005 0551 CDC Laboratory Control Spike 1 05/13/2005 1255 CDC Dilution 1 1 I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-441 J I Fax (864) 229-7119 DAYIS FLtffD LABORATORY ANALYSIS REPORT Client Contact CELANESE 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Richard Ramirez QC Batch Report -Method Blanks Parameter Wot Chemistry SW846 9060 WorkGroup: WG41176 Blank MB41176:l ORGANIC CARBON, TOTAL Result Qual 1.0 NC Certification Number: 25 Project Number: 61621.01 Report Date Page a of 13 Matrix: GW/ChemW June 15, 2005 Report ID: AC1629 RDL Units Analyst Date Time 1.0 mg/1 CDC 05/13/2005 0551 I I I I I I I I I I I I I I I I I I Dav;, ,Hluyd, Inc. I PO Drawer 42/J I Greenwood, SC 2%48 I 816 E. Ducst Avenue I Greenwood, SC 29649 I (B64) 229-4413 I Fax (864) 229-7119 11 I I I I I I I I I I I I I I I I I I I DAYIS FLtJYD LABORATORY ANALYSIS REPORT Client contact CELANESE 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Richard Ramirez NC Certification Number: 25 Project Number: 61621.01 Report Date Page 9 of 13 June 15, 2005 Report ID: AC1629 QC Batch Report -Laboratory Control Standards and Duplicates WorkGroup: WG41176 Matrix GW/ChemW LCS LCS41176:l Prep Method Analtyical Method: SW846 9060 ORGANIC CARBON, TOTAL 25.00 24.86 mg/1 99 90-110 I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-4413 I Fax (8641 229-7119 D~IS FLtJfD LABORATORY ANALYSIS REPORT Client Contact CELANESE 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Richard Ramirez NC Cenification Number: 25 Project Number: 61621.01 Report Date Page 10 of 13 June 15, 2005 Report ID: AC1629 QC Batch Report -Batch Sample List WorkGroup WG41223 Matrix GW/Chemw Description: TOC Prep Method Analtyical Method: SW846 9060 PREP ANALYTICAL Sample ID Client ID Run# Date Time Date Time Analyst L05050602-01 V-23 05/18/2005 1630 CDC MB41223:l Method Blank 1 05/18/2005 1455 CDC LCS41223:1 Laboratory Control Spike 05/18/2005 2056 CDC MS05050901-07 41223 Matrix Spike 1 05/18/2005 1957 CDC MSD05050901-07:41223 Matrix Spike Duplicate 1 05/18/2005 2026 CDC Dilution 200 I I I I I I I I I I I I I I I I I Davb & i:/oyd, Jnc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-4413 I Fax (864) 229-7119 I I I I I I I I I I I I I I I I I I I Dl\VIS FLffl'D LABORATORY ANALYSIS REPORT Client Contact CELANESE 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Richard Ramirez QC Batch Report -Method Blanks Parameter Wet Chemistry SWB46 9060 WorkGroup: WG41223 stank MB412231l ORGANIC CARBON, TOTAL Result Qual < 1.0 NC Cenijication Number: 25 Project Number: 61621.01 Report Date June 15, 2005 Page 11 of 13 Report ID: AC1629 Matrix: GW/ChemW RDL Units Analyst Date Time 1.0 mg/1 CDC 05/18/2005 1455 I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-4413 I Fax (864) 229-7119 DAYIS FLtJYD LABORATORY ANALYSIS REPORT Client Contact CELANESE 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Richard Ramirez NC Certijica1ion Number: 25 Project Number: 61621.01 Report Date Page 12 of 13 June 15, 2005 Report ID: AC1629 QC Batch Report -Matrix Spikes and Duplicates WorkGroup: WG41223 Matrix GW/ChemW M&/MSD MSOS050901-07:41223 Prep Method MSD05050901-07:41223 Analtyical Method: SW846 9060 ORGANIC CARBON, TOTAL 20.00 9. 74 29.14. mg/1 97 74-125 ORGANIC CARBON, TOTAL 20.00 JO.OS 102 3 11 74-125 NOTE: MS/MSD, recoveries are not evaluated if the sample concentration is greater than four times the spike added. I I I I I I I I I I I I I I I I I I Davis & Floyd, Inc. / PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (804) 229-4413 I Fax (864) 229-7119 I I I I I I I I I I I I I I I I I I I Dl\VIS FLtrYD LABORATORY ANALYSIS REPORT Client CELANESE 2525 BLACKSBURG ROAD HWY 198 SHELBY, NC 28152 Contact : Richard Ramirez NC Certification Number: 25 Project Number: 61621.01 Report Date June 15, 2005 Page 13 of 13 Report ID: AC1629 QC Batch Report -Laboratory Control Standards and Duplicates WorkGroup: WG41223 Matrix GW/ChemW LC!S LCS412231l Prep Method Analtyical Method: SWB46 9060 ORGANIC CARBON, TOTAL 25.00 26.22 mg/1 105 90-110 I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2%48 I 816 E. Durst Avenue I Greenwood, SC 29649 I (ll64J 229-4413 I fax {864) 229-71 19 DA,YIS FLtJYD LABORATORY ANALYSIS REPORT Method Conformance Summary Client Celanese -Ticona, LLC, Shelby Plant Login(si L050504 I 0, L05050602 Criteria TOC Sample Holding Time ✓ Standards Preparation ✓ Instrument Tuning ✓ Instrument Calibration ✓ Calibra;ion Verification ✓ Degradation Check NIA Interference NIA SamolelStandard Blanks Results ✓ Method Accuracy ✓ Method Precision ✓ Surrogate Recovery ✓ PDSISDIMSA NIA TCLP Preparation NIA Key ✓ Method Criteria Met NIA Not Applicable • = Method Criteria Not Met -Seefootnote(s) below. PDS = Post Digestion Spike SD = Serial Dilution MSA = Method of Standard Additions Footnotes: Prepared by: ____________ _ Project Number: 61621.01 Report Date: June 15, 2005 I I I I I I I I I I I I I I I I I I D.1vis 8, Floyd. Inc. I PD Drawer 42H I Greenwood, SC 2%411 I H 16 E. Durst Avenue I Creenwood, SC 2%49 I (llf,4) 229-4411 I Fax JH!,4) 229-71 191 -~-- - - - - - - - --SHEALY ENVIRONMENTAL SERVICES, INC. '-. S V Ch · f C t d R d 106 Vantage Point Drive · ,I Bin O US O Y eCOf Cayce, South Carolina 29033 J5 ✓ J.5-,~'tY Telephone No. (803) 791-9700 Fax No. (803) 791-9111 "'50~~1cr Number 16850 - Ghent f:.ug,.j{-Mt', ·tk...Ioc (,(725" Report to Contact ej2, . j::::,,.'~j Q{~ ~'7 u. l. T~hone No.! fax N~. IE-~ . ~-P?2 ·-M9o. f&v-fl:2.-.Jl&J Quote No. Address ·fa fidY ~Ir) 'f 7 S~tuce. ·~ Waybill No. ' Page 1 o,L c;,'.;1,t1-tff"t1NV/1.,,lt: 1. State I Zip Code. , V :Z.,'~.A 7. Analysis (Attach list if more space is needed.) -\ .Sc ;;27£,,J--c, .. Printed Nt,> / PmjectName c•;u4-)t/C,{J,t//f 6 ~ 7.,--01?._7 T;~t/£.4,/pJ 1;( Project No. bLbOS/b P.O. No. ~ I No. of Containers Lot No. !i Matrix by Prese,vative Type Sample ID I Description Date Time l . • 0 M ~ J <:~ ~ Is (Containers for each sample may be combined on one fine.) , I ~ ~f § ~ \l ~ 8 Remarks I Cooler 1.0. < < ~ ~-:}<Y 3/'l/4s' OJ~ Co X I X <->czr~,c cl720c: (35c I / 'I~ .r V I • ✓ ,if== j htf!S I{:, V V _} .,, . I /\ 007-62. -G X: I X If case 'flf,,.z-r I Au ro <. 0,171- 17/tS ?Jo:;zt.T~ OA.J 'T/1: Jb»,4-f'J 7;1~ Jt?,2.J /} Possible Hazard fdentif1CB.tion □ Skin lrrita/,,6~ison Sample Disposal Note: All samples are retained for six weeks from receipt □ Non-Hazard □ Rarpmpble □ Unknown □ Retum to Client L'£Disposal by Lab unless other arrangements are made. Tu~ Aroun~ ~12d (Pnor lab apptl re'quired for expedited TAT) rhtStandard u.c,J,i· (Specify) , / 'oc Requirements (Specify) LGVL~ :JI:. /t. Rehngu~tfy ';//:_ --Dateto//4 Ti/(/?,) 1.-~nv~ I>~ 0 a::z , Time /' lffi-e:-~ -------S; ,,,-~ 14 '?lJ -< 2.TL~is ed~d'-:) / 0 "'/1 in, Time 2. ReceivtJI,, y Date Time ,., .'11Y s 'i -l(,3n 3. Relinquis. Mby Date Time 3'"tis'o;.'ec5-b'w-, '-(;,C0J { ':%. I/. 05 Time 1&:3-o Comments LAB USE ONLY e~ rJ Received on ice (Circle Yes Jee Pack Receipt Temp. "C DISTRIBUTION. WHITE & YELLOW Return to laboratory with Sample(s), PINK F1e/d/C/lent Copy '-- 61f-, ui:rl.LY Chain of Custody Record ,J-t'ft-,,yb Sample ID I Description (Containers for each sample may be combined on one line.) l/✓23 . /I PO. No. Date I ' Possible Hazard Identification / / □ Non-Hazard □,Flammable □ S,J<in lrrit,y,t □ Poison □ Unknown -~ Tu11 Around Tjme V/equired (Prior 1,f> BPP(OVa! required for expedited TAT.) M Standard ~ush (Specify) /,1. / SHEALY ENVIRONMENTAL SERVICES, INC. : 06 Vaniage Point Drive Cayce, South Carolina 29033 Telephone No. (803) 791-9700 Fax No. (803) 791-9111 Waybill No. • No. of Containers o" Matrix by Preservative Type lH Time "0 i " ~ i Ii ~ ~u };: <:~ 8 ~ " ~ u 0 ~, ~ ! ~ 0 "' ._ ~ 0 s 0 (; X I IX L 0...5 ·os-o& o i Number 15·3 4 8 Quote No. ( I Page of-----+- .. Analysis (Attach list if more space is needed.) Lot No. Remarks I Cooler 1.0. fcrAri: ltft.e.,1 /tti ·llG VBJJ /fl.,;1,u 1/fd' ?J,o:;-zz.T,.,, Jb04) /,?v 7?/c )btiJ.97 Sample Disposal □ Return to Client ( Disposal by Lab Note: All samples are retained for six weeks from receipt unless other arrangements are made. / QC Requirements (Specify) -I 5.~o5 Tfrn•o1..3 0 lAB USE ONLY Received on ice (Circle~ No Ice Pack Receipt Temp. .1!.. - --- I I I I I I I I I I I I I I I I I I I . •~)'Y\ (l¾lt.' ·-(},C3, I) I)?-., 0 05 I) CL o,ol- 0/fJ O.o I•. 0.0i I 0.01 0,D/ Lew-Flow Grour.cw-:iter Scmo:ir.g Lo,; Kubal·Furr & Associates Project No. 2(; QS. {(z / Z6 .VA 'ii. ' -[m,iro111111•11f11/ C1m~1i//1111/~ -Site Loco lion CNA/Ticona -Shelby, NC Field Personnel gs . Well I Sample 10 -..f-..~-~2_~'>?~-~-~-c:,· i [! ~ Wea/her Conddion Si,,)'t'.1/~ ~5 5d S Sample Dale --~--'--;/c=../==,---;__:A;::;•ri;,:;;,a;::;I Tim;::;e~ _o_•rrc,_•_,....::.:Sa;::;mp:_:ie:_.::rim:_.::e~ -~(_~1 "';~=:-.f:,=c===,-- Descrip!1on of ,\temuringl ·/eel. ii cc,·,ng T'/pe! (). r•· 11' L-:::cking Cop! / ,! Cosingll ~ i Pcint (MPJI , I rvL c,cme:e1 ,nehei• ::===:::.,_.. _ __;-~~ PvrgeMerhodl ~¼H,\L.-; SomplingMetr",ed/ ~-,,¼J.l-\L I __ Purg'! ':,t~rl [imell 'ooq-i ' PUP;;!<? $loo fime; iD>D j Purge .~ot<:,\.1.,./ /'i.11m.nl Waler-Level Measuremenls Field Parameters fm'1ru) . -(~Cl (~iiL') ~q, (µ$/cm) ln!erval Elapse lime DTW U""et) lnt.,.rval Temperature Speciric Conductance pn (;vJ T\:rt,oity ORP (m\l) 0 I 0 I !s't I 0 I I I I I ' I ' ' I -· I 1'-/S'i~ I 1'5.?o 1 sL/ci I 6, 7,4 I I 3, I z.;,; I _.:..k'c,, /'. I '() I 2 I lo liJ I') g 2 I 15, ~-~ I zdff I I. "'J? I ;7 I z.s-!-i'G,.3 3 I is-!rs. sci 3 I /r;<-',1 s 4) i r. s 3 I l 5 I 1...u [ -7Z< ' I 1o ii S, 5'2 4 I /5,C/ t I 543 ! (_, 3/ I 1 '1 I I,') I-'it/, 5 I ,z,r I !5,7'-i 5 I Jl,. ai./ I 3 L/ I i r . )0 I ·7 r,, I 17.... 1-'1(, Z I YJ I J'J,C/1 I I I., /2-' '?L/0 I r,,, z 'l I 7 0 I I, ':> l-917 I 6 6 I 7 I J,'5 f ,c,_ifi 7 ! /(,, ZJ) ! '.>3'6 I (,,, ZY 137 i 1, r 1-81,7 8 I 4o I ;1o,z1 8 \ 11., l'i I )3G 1. (.,, Z'i, 13 S' I I • l /-fr.ti I 9 I /.fS-I 17 co ' 11&, 24 ! 3 31 I c,,27 1:s"I I J ,o l-tg,1 10 I <;""() ! 17, 70 10 l/fc.17 I ~11 i /,-L llL!t'i I I ,c> f-f'U :S ' II I II I ! I I I 12 I " I ! I I I 13 I 13 I I I I I I /4 I I /4 i I I I I I 15 I I 15 I I I I I I 16 • I I 16 I ! I I I I I 17 I I 17 I I ! I I I I 18 I I " I I ! I I ! I? I I " I I I I I 20 I .:,o I I I \ I I Samples Collected Con101ner Descnp,1on ,. ( X iZ5 inL · j_~:;(cR 1u2::..)2.1 N101~ luff-l~<i R,H-::. zdlcJ:fcf(Y\ > z./.0"'1/L T~rbidi:y +/-IC;; ot>ove 10 NTU +/-I NTU below 10 ,'lTU Oi?P +/• ICmV Ccr,.ve-s;M fa~, I Pf r {1c) •/. n '"'JIL CNA/Ticono Low-FlowGroundwoler Sompijng tog Kubal-Furr & Associate:; -[11t•iiw1111t·irMI C1m,11/tmrl:;- (M1/I--0 I () ! 't,i./'Z-0 -I I C-:' '.) ! q (7 I O,o 2-. 2 I in iq,t,) 2 0102. 3 I I> lq_gcq 3 O,oz. ' I Zo 19,'1 (o ' 0,62. 5 I '2> ! !0167 5 0102 6 I ,O I /0,DY 6 \ 02. C. 7 I 3')\ /fl.A<"° 7 8 1 • 8 ,' 9 I 9 10 I 10 II I II 12 I I 12 13 I I 13 " I " 15 I 15 16 I 16 17 I I 17 18 I I 18 19 I I 19 20 I 20 Somples Collected Low-Flow 'crour,cwcter Sampling Leg P.·ojectNo 2 l°'s I l (2(,)/1.//1. 9'7 Site Location CNA/Ticona -Shelby, NC Field Personnel ~-,{.l,'--=5'-.--c------ We/1 I Sample ID ---cc✓~-=l~s--,,-.,._-,-c=---- S J:,, ~ G,O's / ', ,wzel·therCor.aition ~,~~""'·7'-'.-'--1-+-'~---'1 "' Somo:, T,me _::, .:,__ µ cm ' ' I I I I ' i I ' I I I forbidity (,'ITU) I 1038' ! 4/•7/ I Lf. x'7 I '-I (c Ii/.. 30 I r/20>1 1 'lo i S.& 1 /tc?"7 : i/Zo 7 I 4, °I u I L-1.'- l102LJ ! L/2oi.i IL/.' ll / 3/ I /C, Zl/ 14 I '17 I L/,' 0 I 1-f,G I fl.ZS-I Ll/"/2 I 4."lo l,:z.n I ! I I I ! I I I I I I I I I I I I I I I I I I I I I I I ! I I I I I I I I I I I I I I I I I I I Container D~npt,on Prese1Va1.ve *Dis,olvcd o~ygen ORP (mV) ~.,. '-.C, ' ' ' I ' I I ! i c._, I l~/7 I /,C:, I Lfl.1 I 1 , ~ · I '-/'i 7 I I,-~ I 4g,11 I I. 2.. I '-/7 4 I /. 2 I LI{, 7 I I I I I I I I ! I I ' I I I I I I I ' I I I I I I I I I I z_ 5 • OlA/Ticono low-flowGro,..ndwoter Somp:ir,g log I I I I I I I I I I I I I I I I I I I I I I I Attachment 2 I Selected Water-Quality Plots I I I I I I I I I I I I I Kubal-Furr & Associates ------------------- :::, V-23 TOC Data 14000 ,---------------------------------------------~ (Unfilled data points represent qualified data or values below the detection level.) 12000 -- ------ - ---- - ----- - -- --- - - ---- - - ------- --- ------- - - ------- - - --------- -- ------ --------- - -------- -- - ------ 10000 'o, 8000 E ~ 5 -~ ~ g 6000 8 4000 2000 0-t-----+------+-------t-~------+------+-----+-----1-------+--_J 1/1/85 6/20/87 12/6/89 5/24/92 11/10/94 4/28/97 1 0/1 5/99 4/2/02 9/18/04 Date ------------------- C 0 ~ 1:: 8 C 8 V-23 2-Butanone (MEK) Data 4,--------------------------------------------~ 3.5 3 2 1.5 0.5 (Unfilled data points represent qualified data or values below the detection level.) ---- ---------------- --- ----------------- -------- --------- --- --------- ----- - - - ---------- --- ------------ ---------------------------------------- -------------------------------------------------- ------------------------------------------------------------------------------------------------- 0 +----"'---0----t.,,._,,'--------'=--+-""0----0-+----~::.-----+-----t----------+'ID--O--O--B-+-__J 6/1 /89 6/1/91 5/31/93 5/31/95 5/30/97 Date 5/30/99 5/29/01 5/29/03 5/28/05 ------------------- V-23 Acetone Data 1.4-,---------------------------------------------~ 1.2 0.4 0.2 (Unfilled data points represent qualified data or values below the detection level.) 0+---~~+------+--'-'---_.'+-----+-~-__[J4--------+-----f-O===i~~,E)_+---__J 6/1 /89 6/1/91 5/31/93 5/31/95 5/30/97 Date 5/30/99 5/29/01 5/29/03 5/28/05 ------------------- ~ ..J ' "' E ~ C 0 ., E ., C Q) u C 0 u V-23 Benzene Data 0.3 ,-------------------------------------~ 0.25 0.2 0.15 0.1 0.05 (Unfllled data points represent qualifled data or values below the detection level.) -------------------------------------------------------------------- --------------------------------------------------------------------- ------ - - -------- ---- -- --- - -- ----------------------------------- ------------------------------------------------------------------------ 0 -t------+-----+=-----+----+------+----+------t:1---------+----+.----I 6/1/89 6/1/91 5/31 /93 5/31/95 5/30/97 Sample Date 5/30/99 5/29/01 5/29/03 5/28/05 ------------------- '.J' -;,, K-28 TOC Data 9000 ~-------------------------------------~ (Unfilled data points represent qualified data or values below the detection level.) 8000 ------------ - ----- - -- - - -------- - - - - ------- ------- -- ------ -- - --- - - ----- - ------ - - 7000 -- ------ ---- - - --- - -- - - - - - -- ---- -- -------- -- - ------ -. ------- ----- -- - - ----- - - ------------- --------- 6000 _§, 5000 C: 0 ~ e ~ ~ 4000 8 3000 2000 1000 0 +-------+-------l-----+------+-____:o,. .... ~-~ ............ --~-----1+-11.J-------~ 8/14/81 8/18/84 8/23/87 8/27/90 8/31/93 Date 9/4/96 9/9/99 9/13/02 9/17/05 ------------------- C 0 ., E ~ K-28 Benzene Data 0.035 ,----------------------------------------------~ 0.03 0.025 (Unfilled data points represent qualified data or values below the detection level.) g 0.01 5 0 u 0.01 0.005 0+------+--------1-----+------+-----t--------+-------+-----+---_J 6/1/89 6/1/91 5/31/93 5/31 /95 5/30/97 Date 5/30/99 5/29/01 5/29/03 5/28/05 ------------------- C 0 ., ~ C ., u C HH-48 TCE Data 0.25 ,-----------------------------------------------~ 0.2 (Unfilled data points represent qualified data or values below the detection level.) 8 0.1 0.05 0+------------+-----+------l--------+------+------+------e--J 6/30/89 6/30/91 6/29/93 6/29/95 6/28/97 Date 6/28/99 6/27 /01 6/27/03 6/26/05 ------------------- HH-77 TCE Data 0.5 -,------------------------------------------~ 0.45 0.4 0.35 (Unfilled data points represent qualified data or values below the detection level.) ------------------------------------------------------------------------------------------- ---- ---------- - - ------ -- - - - ------ --- ---- -------- -------- ------ - ----- ---------------------------------------------------------------------------- C 0 -~ 0.25 .., C fl C 8 0.2 0.15 0.1 0.05 --------------------------------------------------------------------- 0+------+-----t-----f--------1-----+------+-----+------+__J 6/1/89 6/1/91 5/31/93 5/31/95 5/30/97 Date 5/30/99 5/29/01 5/29/03 5/28/05 I I I I I Attachment 3 I CD ROM of Semiannual Report In pdf Format I (Back Cover) I I I I I I I I I I I I Kubal-Furr & Associates