HomeMy WebLinkAboutNCD003446721_20050627_Celeanse Corporation - Shelby Fiber_FRBCERCLA RA_OU-1 Semiannual Report January - June 2005-OCRI
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Post Office Box 2732 IO
Tampa, FL 33688-32IO
8 I 3-265-2338
FAX-265-3649
Mr. Kenneth A. Lucas
U.S. EPA Region IV
Atlanta Federal Center
6 I Forsyth Street
Atlanta, GA 30303-8960
Kubal-Furr & Associates
Environmental Management Services
July 27, 2005
Re: OU-I Semiannual Report-Ticona, Shelby-January 2005-June 2005
Dear Ken:
Post Office Box 80247
Simpsonville, SC 29680-0247
864-962-9490
FAX-962-5309
On behalf of CNA Holdings, Inc., we are pleased to enclose two copies of the report entitled: "Operable Unit
I-Semiannual Report-January 2005-June 2005-CNA Holdings, lnc.-Shelby, North Carolina." By way of this
letter, we have also transmitted a copy of the report to David Mattison with NCDENR for his review.
Please contact me at 813-265-2338, to discuss any questions you may have following your review of this
document.
Sincerely,
Kubal-Furr & Associates
Jz/{;__~-
Jerry E'. Kubal, P.G.
President
cc: David Mattison, DENR
Rick Ramirez, Celanese Americas
PEM Carter, Ticona
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CNA Holdings, lnc./Ticona-Shelby, NC-Ql IQ2 2005 Semiannual Report I Page i
Contents
Page
Acronyms/ Abbreviations ............................................................................................................................ .iii
1.0 Introduction .......................................................................................................................................... I
2.0 Work Performed ................................................................................................................................... 3
2.1 1st Quarter 2005 ........................................................................................................................... 3
2.2 2nd Quarter 2005 ......................................................................................................................... 4
2.3 Free Product DowTherm®A Bailing-Well F-55 .................................................................... 4
3.0 Discussion of Findings ......................................................................................................................... 5
3.1 Ground-Water Movement ........................................................................................................... 5
3.2 Ground-Water Quality ................................................................................................................. 5
3.3 Discussion of Analytical Test Results ........................................................................................ 6
4.0 Review of Selected Historical Water-Quality Data ........................................................................... 8
5.0 Closing Comments .............................................................................................................................. IO
Tables
Table I. 2005 Sampling Matrix-CNA Holdings, Inc.-Shelby, NC
Table 2. Summary of Selected CERCLA-Related Water-Quality Data-(lst Quarter 2005)
Table 3. Summary of Selected CERCLA-Related Water-Quality Data-(2nd Quarter 2005)
Table 4. Summary of Selected PEW-Related Water-Quality Data-( I st Quarter 2005)
Figures
Figure I. Site Location Map-CNA Holdings, Inc./Ticona-Shelby, NC
Figure 2. Potentiometric Surface Map-Shallow Saprolite-February 10, 2005
Figure 3. Potentiometric Surface Map-Deep Saprolite/Upper Bedrock-February 10, 2005
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CNA Holdings, lnc./Ticona-Shelby, NC-QJ/Q2 2005 Semiannual Report I Page ii
Figure 4. Hydrogeologic Cross Section-February IO, 2005
Figure 5. Potentiometric Surface Map-Shallow Saprolite-May 2, 2005
Figure 6. Potentiometric Surface Map-Deep Saprolite/Upper Bedrock-May 2, 2005
Figure 7. Hydrogeologic Cross Section-May 2, 2005
Attachments
Attachment 1. Analytical Data Package, Data Assessment Summary and Field Sampling Logs for the
!st and 2nd Quarter 2005 Sampling Events
Attachment 2. Selected Water-Quality Plots
Attachment 3. Back Cover-CD ROM of Semiannual Report in pdf Format
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CERCLA
CFO
CNA
DENR
EPA
ESD
Fil
FP
GC/FID
!MAC
ITC!
ITEF
LTRA
MCL
MEK
mg/L
MNA
NFG
NPL
OTC!
OTEF
OU-I
OU-2
PCE
PEW
ROD
SBR
svoc
TCE
TCLP
TOC
voe
CNA Holdings, Inc./Ticona-Shelby, NC-Ql/Q2 2005 Semiannual Report I Page iii
Acronyms/Abbreviations
Comprehensive Environmental Response and Liability Act
Celanese Fiber Operations
CNA Holdings, Inc.
(North Carolina) Department of Environment and Natural Resources
U.S. Environmental Protection Agency
Explanation of Significant Differences
Fiber Industries, Inc.
Filter Press
Gas Chromatograph/Flame Ionization Detector
Interim Maximum Allowable Concentration (North Carolina)
Inner Tier Combined Influent
Inner Tier Effluent
Long Term Remedial Action
Maximum Contaminant Level
Methyl Ethyl Ketone (2-Butanone)
Milligrams per Liter
Monitored Natural Attenuation
National Functional Guidelines (for organic/inorganic data review)
National Priorities List
Outer Tier Combined Influent
Outer Tier Effluent
Operable Unit I
Operable Unit 2
Tetrachloroethene
Polymer Extraction Well
Record of Decision
Sequencing Batch Reactor
Semivolatile Organic Compound
Trichloroethene
Toxicity Characteristic Leaching Procedure
Total Organic Carbon
Volatile Organic Compound
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CNA Holdings, lnc.!Ticona-Shelby, NC-Ql/Q2 2005 Semiannual Report I Page I
1.0 Introduction
Ticona, an operating subsidiary of Celanese, owns and operates a polyester and engineering plastics
production facility in Shelby, North Carolina. CNA Holdings, Inc. (CNA), also a subsidiary of Celanese,
retains management of environmental matters for the corporation and thus, is responsible for the work
performed during the semiannual reporting period. The Shelby site consists of an approximate 450-acre
piece of property which includes the main plant production area, wastewater treatment area, former waste
disposal areas, and recreational areas. The plant is located in south central Cleveland County, bordered by
NC Highway 198 to the west and Lavender Road to the south, approximately one mile north of Earl and
six miles south of Shelby. A site plan showing the location of production areas, monitor wells, extraction
wells, and other significant features is shown on Figure I.
Operations at the site began in 1960 by Fiber Industries, Inc. (Fil), a manufacturer of polyester chips
and filament yarn. Celanese Corporation bought the facility from Fil in 1983, renaming it Celanese Fiber
Operations (CFO), and continued the production and processing of polyester polymer chips and fibers.
The site has alternately been known as HNA Holdings, Inc., Hoechst Celanese Corporation, and Celanese
Fiber Operations, the latter being the site name as listed on the National Priorities List (NPL).
CNA currently maintains a long term remedial action (L TRA) system at the CFO site, designated as
Operable Unit I (OU-I) in the Record of Decision (ROD). OU-I consists of two ground-water extraction
and treatment systems identified as the Inner Tier and Outer Tier systems. OU-I became operational in
August of 1989. A second operable unit, OU-2, consisted of excavation, incineration and reburial of
stabilized incinerator ash and other inert waste materials. Current status of the OU-I LTRA is discussed
below.
On April 21, 1998, OU-2 and the Outer Tier portion of OU-I were shut down as part of a partial
delisting petition approved by the EPA effective April 17, 1998. Further, implementing EPA
recommendations in the August 200 I Five-Year Review Report, the Inner Tier was shut down on March
I, 2004 while CNA implements and evaluates an MNA (monitored natural attenuation) demonstration
project.
·· The entire Outer Tier is being maintained in "standby status" as part of the delisting process and can
be brought on-line within a relatively short period of time if it is found necessary to provide hydraulic
control along the property boundary. The Outer Tier wells functionality is assured by performing routine
monthly and quarterly system checks such as energizing the well pumps, transfer pumps and blowers,
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CNA Holdings, Inc./Ticona-Shelby, NC-QJ!Q2 2005 Semiannual Report I Page 2
verifying heater operation, etc. and performing maintenance activities as required by the routine system
checks.
With an effective date of April 23, 2004, an ESD (Explanation of Significant Differences) was
utilized to modify selected elements of the remedial alternatives contained in the OU-I ROD. The ESD
provides for CNA to discontinue treatment of recovered ground water in a separate ground-water
treatment system (consisting of a sequencing batch reactor [SBR], air stripping and carbon polishing) and
instead to reroute recovered ground water to the existing industrial wastewater treatment plant. This
modification is scheduled to take place following review of the outcome of the MNA demonstration
project at which time a decision will be made as to the need to restart the Inner Tier recovery well system.
Currently, CERCLA-related (Comprehensive Environmental Response and Liability Act) LTRA
monitoring activities consist of quarterly sampling of selected monitor wells (Table I) and submittal of
semiannual reports to the EPA (Environmental Protection Agency) and DENR (State of North Carolina
Department of Environment and Natural Resources). Non-CERCLA semiannual sampling of PEW wells
(polymer extraction wells) also takes place and these data are submitted along with the routine
semiannual CERCLA reports. Samples are also collected quarterly from selected monitor and extraction
wells as part of the MNA demonstration project and are reported separately to the agencies in the form of
quarterly data collection reports.
Kubal-Furr & Associates (Kubal-Furr) has prepared this semiannual OU-I operating summary report
for submittal to the EPA and DENR on behalf of CNA. It covers the period from January I, 2005 through
June 30, 2005 and includes the results of analytical testing of samples collected during the periods
February 15-23, 2005 and May 4, 2005.
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CNA Holdings, Inc./Ticona-Shelby, NC-QJIQ2 2005 Semiannual Report I Page 3
2.0 Work Performed
As part of the OU-I remedy, CERCLA-related samples are collected at selected monitor wells and
analyzed for the parameters summarized in Table I. In addition, samples are collected from the inactive
PEW system and selected PEW-related monitor wells. The location of all monitor and extraction wells is
shown on Figure I. A description of the work performed during this reporting period is provided below.
2.1 1st Quarter 2005
On February IO, 2005, water levels were measured by Kubal-Furr in a total of I 16 monitor wells,
extraction wells, and piezometers. A total of 13 CERCLA-related ground-water quality samples were
collected during the period February 15-23, 2005, in accordance with the sampling matrix shown in Table
I. All samples were collected by Kubal-Furr and analyzed by Davis & Floyd Laboratories of Greenwood,
South Carolina.
OU-1 Monitor Well Sampling
Thirteen monitor well samples were collected using low-flow sampling protocols. The samples were
analyzed in the field for pH, temperature, conductance, turbidity, dissolved oxygen (DO) and oxidation
reduction potential (ORP); and, by the laboratory for volatile organic compounds (VOCs) using EPA
Method 82608. In addition to analysis of volatiles, samples from monitor wells V-23 and K-28 were
analyzed by the laboratory for total organic carbon (TOC) using EPA Method 9060.
PEW Extraction and Monitor Well Sampling
Three PEW grab samples (PEW-I, PEW-3, and PEW-4) and one monitor well sample (F-55) were
collected during the I st Quarter. These samples were analyzed in the field for pH, temperature,
conductance, turbidity, DO and ORP; and, in the laboratory for VOCs by EPA Method 82608 and for
SVOCs (semivolatile organic compounds) by EPA Method 8270C (including the DowTherm®A
constituents I, 1-biphenyl and bi phenyl ether).
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CNA Holdings, lnc.!Ticona-Shelby, NC-Ql!Q2 2005 Semiannual Report I Page 4
2.2 2nd Quarter 2005
On May 2, 2005, water levels were measured by Kubal-Furr in a total of I 16 monitor wells,
extraction wells, and piezometers. Water-quality samples were collected from two monitor wells (V-23
and K-28) and were collected on May 4. 2005 by Kubal-Furr and analyzed by Davis & Floyd. These
wells were analyzed in the field for pH, temperature, conductance, turbidity, DO and ORP; and, by the
laboratory for TOC by Method 9060.
2.3 Free Product DowTherm®A Bailing-Well F-55
As discussed in earlier semiannual reports, free product DowTherm®A was found to be accumulating
in monitor well F-55 following a monitor well rehabilitation program implemented in September 200 I.
Prior to the current semiannual reporting period, well F-55 was sounded/bailed on 15 separate occasions
since March of 2002 and the total volume of DowTherm®A recovered was approximately 2.43 gallons
(9.19 liters). Well F-55 was bailed during the 1st and 2nd Quarters and 0.23 gallons (0.88 liters) of free
product was recovered (0.13 gallons [0.49 liters] and 0.10 gallons [0.39 liters] in the I st and 2nd Quarters,
respectively), bringing to 2.66 gallons (10.07 liters) the total amount of DowTherm®A recovered to date.
This well will be tested again in the 3rd and 4th Quarters of 2005 and any free product accumulations will
be removed and recorded.
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CNA Holdings, lnc.!Ticona-Shelby, NC-Ql/Q2 2005 Semiannual Report I Page 5
3.0 Discussion of Findings
3.1 Ground-Water Movement
As previously discussed. water levels were collected on February 10, 2005 by Kubal-Furr, and again
on May 2, 2005. These data were used to construct potentiometric surface maps and hydrogeologic cross
sections (Figures 2 thru 7).
The shallow saprolite maps (Figures 2 and 5) show water-level contours and direction of ground
water movement in the uppermost water-bearing zone beneath the site. The direction of movement in this
zone is to the east, northeast and southeast from upgradient areas along NC 198, towards discharge areas
along the unnamed tributaries of Buffalo Creek.
An attempt was made to separate the uppermost water-bearing zone from the deeper saprolite and
upper bedrock zone. While these maps (Figures 3 and 6) present a reasonable picture of ground-water
movement in this zone, it should be pointed out that it is giving a more generalized picture of ground-
water movement because of the well construction techniques used in many of the wells and piezometers.
The typical construction of these wells was to have relatively long screens and extremely long sand packs
in the annular space above the screens. As a result, the lower saprolite/upper bedrock maps have a number
of composite head values measured along a longer screened area. However, the maps may be useful for
determining the general direction of ground water movement.
Hydrogeologic cross sections were also constructed from the February and May data sets (Figures 4
and 7). The location of the cross section is shown on the site location map, Figure I. The east-west cross
section (A-A') is constructed through the plant and indicates flow is predominantly horizontal across the
site, from up gradient areas west of the plant toward downgradient areas to the east.
3.2 Ground-Water Quality
The analytical data for the I st and 2nd Quarters of 2005 were evaluated using method specific quality
control criteria and, for additional guidance when necessary, the EPA's National Functional Guidelines
(NFG) for organic and inorganic data review.
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CNA Holdings, lnc.!Ticona-Shelby, NC-Ql/Q2 2005 Semiannual Report I Page 6
The I st and 2nd Quarter data were considered quantitative with several exceptions as noted in the
Data Assessment Summaries (Attachment I). Based on the data-quality assessment, qualifiers were.
placed on selected analytical results as noted in Tables 2 and 4.
Acetone was detected in the field blank collected on 2/22/05 at a concentration of 0.016 mg/L.
Consequently. the acetone for sample P-58 was flagged with a "U" qualifier as non-detect. The phenol
result for field sample F-55 was flagged with a "J" qualifier as estimated, due to low recovery of
surrogate and recovery values for phenol in the associated matrix spike/matrix spike duplicate samples
that exceeded control limits. Benzene, methylene chloride and toluene results from well F-55 were
assigned an "X" qualifier by the laboratory to indicate a higher reporting limit due--}matrix interference.
The X qualifier had no affect on..latl1iusability .
.(J-._
3.3 Discussion of Analytical Test Results
Analytical test results, field sampling logs, and chain-of-custody forms for the I st and 2nd Quarter
data sets are contained in Attachment I. A summary of selected analytical data for the I st and 2nd
Quarters is presented in Tables 2, 3 and 4.
CERCLA-Monitor Wells
Of the 13 CERCLA-monitor well samples analyzed during the reporting period, 6 had volatile
organics reported above the detection level (Table 2). Of these six, three (V-23, CC-33, and K-28) had
two or more individual volatile constituents reported as present above the detection level. The most
frequently reported volatiles included trichloroethene (TCE) (three detects), and benzene and toluene (at
two detects each).
Monitor wells V-23 and K-28 reported the largest number of individual volatiles at four each. V-23
reportedly contained benzene (0.021 mg/L), ethylbenzene (0.003 I mg/L), toluene (0.0 IO mg/L), and total
xylenes (0.012 mg/L). K-28 reportedly contained 2-butanone (MEK) (0.084 mg/L), acetone (0.12 mg/L),
benzene (0.0083 mg/L), and toluene (0.0020 mg/L). CC-33 reportedly contained two volatiles
(chlorobenzene at 0.0019 mg/L, and cis-1,2-dichloroethene at 0.0022 mg/L). T-35, HH-48 and HH-77
reported the presence of one volatile, TCE, at 0.0016 mg/L, 0.20 mg/L, and 0.38 mg/L, respectively.
Benzene and TCE were the only constituents reported above a North Carolina 2L ground-water quality
standard (two instances each).
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CNA Holdings, Inc.!Ticona-Shelby, NC-QJ/Q2 2005 Semiannual Report I Page 7
Monitor wells K-28 and V-23 were also analyzed for TOC during the 1st and 2nd Quarters. K-28 was
reported to contain 60.4 mg/L and 52.7 mg/L TOC during the I st and 2nd Quarters, respectively. V-23.
was reported to contain 10,700 mg/Land 8,900 mg/L TOC during the 1st and 2nd Quarters, respectively.
PEW-Related Samples
Four PEW-related samples were collected during the I st Quarter. No volatiles were reported as
present in the sample from PEW-3. PEW-I reportedly contained the volatiles cis-1,2-dichloroethene
(0.0012 mg/L), chloroform (0.0016 mg/L) and trichloroethene (0.0055 mg/L). PEW-4 reportedly
contained the volatiles benzene (0.0026 mg/L), cis-1.2-dichloroethene (0.0056 mg/L) and trichloroethene
(0.015 mg/L). F-55 was reported to contain the volatiles benzene (0.051 mg/L), methylene chloride
(0.014 mg/L), and toluene (0.0057 mg/L).
Three of the four PEW-related samples (F-55, PEW-3 and PEW-4) had reportable quantities of
DowTherm®A constituents (i.e., 1,1-biphenyl or biphenyl ether). I, 1-Biphenyl was reported as present in
well F-55 (20.8 mg/L) and PEW 3 (0.27 mg/L). Biphenyl ether was reported as present in F-55 (62.7
mg/L), PEW-3 (0.86 mg/L) and PEW-4 (0.026 mg/L).
Benzene, methylene chloride, TCE, 1, I bi phenyl and 2-methylnaphthalene were the constituents
reported above a North Carolina 2L ground-water quality standard. Well F-55 reportedly contained the
largest number of constituents at seven, and the largest number above a 2L standard at four (benzene,
methylene chloride, I ,I biphenyl and 2-methylnaphthalene). PEW-4 reportedly contained four
constituents, two above a 2L standard (benzene and TCE). PEW-I reportedly contained three
constituents, with one above a 2L standard (TCE). PEW-3 reportedly contained two constituents, with
none exceeding a 2L standard.
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CNA Holdings, Inc.!Ticona-Shelby, NC-QJ/Q2 2005 Semiannual Report I Page 8
4.0 Review of Selected Historical Water-Quality Data
Attachment 2 contains plots of water-quality constituents for selected monitor wells. The choice of
locations and constituents was based on a review of the water-quality database, in particular those
locations having any meaningful data to plot. In general, only those monitoring locations within a few
hundred feet of the former OU-2 source area have any significant number of water-quality constituents
reported above the detection limits. In order to assess long-term trends and improvement in water-quality
conditions resulting from source removal and prior ground-water recovery, the following locations and
constituents were selected for review:
• Monitor Well Y-23 TOC, 2-butanone (MEK-methyl ethyl ketone), acetone and benzene data. The
V-23 TOC concentrations began trending downward from a high of 8,000 mg/Lin mid-1989 to less
than 1,000 mg/L in early 1992. Since that time, the TOC data have shown several wide swings in
concentration, with it not being uncommon to note quarter-to-quarter changes of more than 4,000
mg/L. Since 1996, the TOC values have generally fluctuated in the range of 3,000 mg/L to over
12,000 mg/L, although the most recent 2nd Quarter 2005 value of 8,900 mg/L represents the lowest
TOC reported in the previous seven quarters.
The V-23 MEK data have generally fluctuated in a narrow range below I mg/L, and the last 16
sample results have all been reported below 0.5 mg/L, with the last 5 quarterly samples reported
below detect. The V-23 acetone test results had generally been oscillating between 0.2 mg/Land 0.5
mg/L for the past four years, however, the last four quarterly samples have been reported below the
detection level of 0.0050 mg/L.
While more than half the benzene data for Y-23 are flagged as estimated or below the detection
limit, 18 of the past 22 sampling events have been quantitative and show benzene to be fluctuating in
a narrow range of from 0.01 to 0.03 mg/L.
• Monitor well K-28 TOC and benzene data. TOC and benzene have both shown a steady decrease
in concentration beginning about the time the OU-2 source remediation began in January of 1991.
The TOC concentrations at K-28 have shown several wide swings in concentration up to 2,710 mg/L
during the past three years and these increases may be related to a combination of a well rehabilitation
program undertaken in 2001 and shutting down the Inner Tier extraction wells. The most recent two
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CNA Holdings, lnc./Ticona-Shelby, NC-QJIQ2 2005 Semiannual Report I Page 9
quarters (I st and 2nd Quarter 2005) were reportedly back down to pre-200 I levels (at 60.4 mg/L and
52.7 mg/L, respectively).
Although benzene had also shown a general decline since OU-2 source remediation, the
concentrations had increased since the 2nd Quarter of 2003 from 0.0057 mg/L to 0.0 I I mg/L during
the I st Quarter of 2004. The most recent sample for benzene at K-28 (I st Quarter of 2005) was
reportedly back down to 0.0083 mg/L.
• Monitor well HH-48 and HH-77 TCE data. The HH-48 TCE test results had shown a decline
from 0.222 mg/L in August of 1995 to less than 0.1 mg/L during the 3rd Quarter of 2000. Since that
time, TCE concentrations at HH-48 had steadily increased to a 3rd Quarter 2003 value of 0. I 9 mg/L.
TCE receded between the 3rd Quarter 2003 and I st Quarter 2004 but was noted to increase again
between the I st and 3rd Quarters of 2004 and the I st Quarter of 2005.
TCE at HH-77 had been trending upward between 1989 and 1996 when it peaked during July
1996 at 0.383 mg/L. TCE at HH-77 subsequently decreased substantially to 0.059 mg/L during the
I st Quarter of 200 I, however, the concentration was noted to increase during the 3rd Quarter of 200 I
(0.35 mg/L) and to achieve a high of 0.46 mg/L during the 3rd Quarter of 2002. The 3rd Quarter 2003
concentration of TCE at HH-77 had reportedly receded to less than 0.05 mg/L, its lowest level since
1990, but during the I st Quarter 2004, the concentration rose again to 0.31 mg/L and during the 3rd
Quarter 2004 achieved a historic high of 0.47 mg/L. The TCE at HH-77 has since receded to 0.38
mg/L ( I st Quarter of 2005).
The presence of TCE at these locations (HH-48 and HH-77) are thought to be the result of a
localized source on the former Elliott property, unrelated to activities at CNA/Ticona or the former
OU-2 source area.
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CNA Holdings, Inc./Ticona-Shelby, NC-QIIQ2 2005 Semiannual Report I Page IO
5.0 Closing Comments
The current report presents the results of quarterly CERCLA-related and semiannual PEW-related
ground-water sampling at the CNA/Ticona Shelby, NC facility. The next round of samples are scheduled
to be collected during the 3rd and 4th Quarters of 2005 and will be included in the next semiannual report
to the agencies in March 2006.
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Table 1. 2005 Sampling Matrix-CNA Holdings, lnc./Ticona-Shelby, NC
1st Quarter
Monitoring Toe voe
Location (9060) (82608)
Monitor We/Js
C-49 .,J
K-28 .,J .,J
P-58
T-35 .,J
V-23 .,J .,J
AA-54
CC-33 .,J
EE-58 .,J
FF-34
FF-62 .,J
GG-61 .,J
HH-48
HH-77 .,J
PEW-Related Same/es
PEW-1 .,J
PEW-3 .,J
PEW-4 .,J
F-55
Notes:
TOC = Total Organic Carbon
VOC ::: Volatile Organic Compounds
SVOC = Semivolatile Organic Compounds
PEW = Polymer Extraction Well
9060/8260B/8270C = Test methods in SW846
2nd Quarter 3rd Quarter
svoe Toe voe svoe Toe voe svoe
(8270C) (9060) (82608) (8270C) (9060) (8260B) (8270C)
.,J
.,J .,J .,J
.,J
.,J .,J .,J
.,J
.,J
.,J
.,J
.,J
.,J .,J .,J
.,J .,J .,J
.,J .,J .,J
- - - -
4th Quarter
Toe voe SVoe
(9060) (8260B) (8270C)
.,J
.,J
CNA Holdings, lnc./Ttcona-Shelby, NC
OU-I Semiannual Report (Jan. '05 June '05)
-
- - - - -- - - - - - - - - -
Table 2. Summary of Selected CERCLA-Related Water-Quality Constituents (1st Quarter 2005)
CNA Holdings, lnc./Ticona-Shelby, North Carolina
(All results reported in milligrams per liter [mg/L])
Total Organic Carbon
Volatile Organics
2-Butanone (MEK)
Acetone
Benzene
Cis-1 , 2-Dichloroethene
Chlorobenzene
Ethyl benzene
Toluene
Trichloroethane
Xylenes (total)
EPA/NC P-58 ✓
NE/NE NA
NE/4.20 <0.0050
NE/0.7 0.0091U ·
0.005/0.001 <0.0010
0.0710.07 <0.0010
0.1 /0.05 <0.0010
0.7/0.550 <0.0010
1.0/1.0 <0.0010
0.005/0.0028 <0.0010
10/0.53 <0.0020
Notes: NA = Sample not analyzed for indicated constituents
T-35 / V-23 /
NA 10700
<0.0050 <0.0050
<0.0050 <0.0050
<0.0010 0.021 ·
<0.0010 <0.0010
<0.0010 <0.0010
<0.0010 0.0031 •
<0.0010 0.010 '
0.0016 <0.0010
<0.0020 0.012 '
EPA = Environmental Protection Agency National Primary Drinking Water Standards
K-28 /
0.084 ·
0.12 ·
0.0083 ·
<0.0010
<0.0010
<0.0010
0.0020 ·
<0.0010
<0.0020
NC = North Carolina Groundwater Quality Standards ( 1 SA NCAC 02L .0202 [April 1, 2005])
NE = Not Established
U = Constituent not detected above the associated sample quantitation limit
CC-33 /
NA
<0.0050
<0.0050
<0.0010
0.0022 ·
0.0019·
<0.0010
<0.0010
<0.0010
<0.0020
- - -
HH-48 / HH-77 /
NA NA
<0.0050 <0.01 5
<0.0050 <0.01 5
<0.0010 <0.0030
<0.0010 <0.0030
<0.0010 <0.0030
<0.0010 <0.0030
<0.0010 <0.0030
0.20 0.38
<0.0020 <0.0060
CNA Holdings, lnc.mcona-Shelby, NC
OU-1 Semiannual Report (Jan. '05 -June '05)
-
- -- -- - - - - - - -- --- - -
Notes:
Table 3. Summary of Selected CERCLA-Related Water-Quality Constituents (2nd Quarter 2005)
CNA Holdings, lnc./Ticona-Shelby, North Carolina
(All results reported in milligrams per liter [mg/L])
EPA/NC
Total Organic Carbon NE/NE
K-28/
52.7
DUP-2
(K-28)/
50.1
EPA = Environmental Protection Agency National Primary Drinking Water Standards
NC = North Carolina Groundwater Quality Standards (Subchapter 2L)
NE= Not Established
V-23 ./
8900
CNA Holdings, lncflicona-Shelby, NC
OU-1 Semiannual Report (Jan. '05 -June '05)
-
- - ----- - - - - - -- - -
Table 4. Summary of Selected PEW-Related Water Quality Constituents (1st Quarter 2005)
CNA Holdings, lnc./Ticona-Shelby, North Carolina
(All results reported in milligrams per liter [mg/L])
EPA/NC F-55 / PEW-1 ✓
DUP-4
(PEW-1)✓ PEW-3 /
Semivo/atile Organics
1 , 1 Biphenyl NE/0.35 20.8 · <0.010 <0.010 0.27 ·
2-Methylnaphthalene NE/0.0140 0.074 , <0.010 <0.010 <0.010
Biphenyl Ether NE/NE 62.7 · <0.010 <0.010 0.86 ·
Phenol NE/0.30 0.26J · <0.010 <0.010 <0.010
Volatile Organics
Benzene 0.005/0.001 0.051X, <0.0010 <0.0010 <0.0010
Chloroform 0.08/0.07 <0.0030 0.0016 0.0018 • <0.0010
Cis-1,2-Dichloroethene 0.07/0,07 <0.0030 0.0012 0.0012 , <0.0010
Methylene Chloride 0.005/0,0046 0.014X • <0.0010 <0.0010 <0.0010
Toluene
Trichloroethene
Notes:
1.0/1.0 0.0057X · <0.0010 <0.0010 <0.0010
0.005/0.0028 <0.0030 0.0055 0.0054 • <0.0010
EPA = Environmental Protection Agency National Primary Drinking Water Standards
NC= North Carolina Groundwater Quality Standards (15A NCAC OZL .0202 [April 1, 2005))
NE= Not Established
DUP = Duplicate Sample
J = The analyte was positively identified; the associated numerical value is the approximate
concentration of the analyte in the sample.
X = Sample diluted due to matrix interference (applied by the laboratory), no affect on data useability
- - - -
PEW-4 /
<0.010
<0.010
0.026 ·
<0.010
0.0026 ·
<0.0010
0.0056
<0.0010
<0.0010
0.015
CNA Holdings. /nc.fficona-Shelby, NC
OU-I Semiannual Reporr (Jan. '05 -June '05)
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--
..
•0
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- - -- - -- - - -
0 350 700
- - - - - -
Legend
• MonitorWeff
4 Piezomet&r
• Surface Water Location
• Outer Tier Extraction Well
• Inner Tier Extraction Wen
■ PEW Extraction Well
a Residential Well
,,,,,--.,," Creek/Stream
□ Building I Structure
Kubal-Furr & Associates
-Environmental Consultants-
Figure 1. Site Location Map
C.\~ Holdings, lncfficono
Shelby, Nonh Carolina
-
-- -
I
0
•
0
Legend
MnnttnrWell Water-Level (ft msl)
• Inner Tier Extraction Well
,,,,,-...--,, Creek/ Stream
(E Building I Structure
Inferred Direction of Ground-Water Flow
- - -- -
' ' ,. --\
I , '
Recreation Pond
-
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Water-I eve! Elevations
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IT-1 = 804.21
IT-2 = 805.25
IT-3 = 802.94
IT-4 = 802.59
IT-5 = 803.74
IT-6 = 804.08
IT-7 = 803.82
IT-SR = 800 .54
IT-9 = 798.05
Kubal-Furr & Associates
-Environmental Consultants-
Figure 2. Potentiometric Surface Map
Shallow Saprolite-February 10, 2005
C\~4 Holdings, lnc.1Ticona
Shelb)•, l'l/orth Carolina
-- -- ------ - --
' ,. , -. ' I
I
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~ '
, ., ..... ~ L
\
' ofs~~ 'J \\ \. ..
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0 350 700
-
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- - --
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Legend
"'"""'-"'ell Water-Level (ft msl)
Piezometer
❖ Outer Tier Extraction WeB
■ PEW Extraction Well
/780/ W~~t.i:!~ur
,,.-..-,, Creek/ Stream
□ Buikllng I Structure
..,...,, Inferred Direction of Ground-Water Flow
• Water level for well F-55 was
measured on 2/18/05
Kubal-Furr & Associates
-Environmental Consultants~
Figure 3. Potentiometrlc Surface Map
-
Deep Saprolite/Upper Bedrock-February 10, 2005
CNA Holdings, /nc.!Ticona
Shelby, North Carolina
- - - - - - - - - - - ---
850.00 A -~ •~=--=--=--=--=--=--=--=--=--=--~--:~la~nt~A<~•~•:.::=======~r=:::::;:::----------'VVastewater Treatment A.rea------------e
830.00
810.00
79000
770.00
750.00
730.00
710.00
690.00
670.00
D-66
827.16
,-;,. A,.,._
A A;. A,. A;,. ;. A A,.,.,.,. ,. ,. ,. ,. ,. ,. ,. ,. ,. ,. ,. ,. ,. ,. ,. ,. ,. ,.
Legend
-8101 Une of equal fluid potential (ft msl) GJ Bedrock
(dashed 'Mlel'e rnerred)
• -Potentiometric Surface Saprolite
G-50
813.61
Inferred direction of ground-water movement
Screened Interval of V\lell
J-29
808.12
Horizontal Scale in Feet
0 400 800
'-
• C ::J
i,'
!
I
GG-25
754.51"" I GG-39
754.25
- - - -
A' 650.00
830.00
810.00
790.00
770.00
750.00
730.00
710.00
691100
670.00
Kubal-Furr & Associates
-Environmental Consultants -
F1gure 4. HJdrogeologlc Cross Section
A-A'-February 10, 2005
CNA Holdings. lncfficona
Shelby. North Carolina
-
- - -
0
I
0
0
Legend
MoottorWell
Water-level (n fMI)
• Jnner Tier Extraction Well
/?so/ ~~~v:!=ur
..,,,-...-,, Creek I Stream
Iii Building/ Strucll,mt _,,, Inferred Direction of
Ground-water Flow
--- ---- -
', .. - -I
. ' I
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\
' '
~~ m~
\
.... -· .. •
1 II ~1 R,_wn
c=i7ii~ ~,™o,
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0 350 700
- - -
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- - - - -
Inner Der Extraction Well
Water-I eve! Elevations
I
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IT-1 = 805.30
IT-2 = 806.24
IT-3 = 803.60
IT-4 = 803.33
IT-5 = 804.24
IT-6 = 804.65
IT-7 = 804.53
IT-SR= 800.12
IT-9 = 798.63
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I., ..., I, ~ ' . -I '.
Kubal-Furr & Associates
-Environmental Consultants-
Figure 5. Potentiometric Surface Map
Shallow Saprolite-May 2, 2005
CNA Holdings. Jnc.!Ticona
Shelby, North Carolina
- - - - - -- - - - - -
\
-
?. •,
' ,
' , ,.
e ' I ,
I>
I
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Recreation Pond
o~:
---~\
0 ,00
- - - - --Legend
Moaimr Well 0 Water-level (ft msl) ... Piezometer
❖ 0ut8f ner Extraction Well
■ PEW Extraction Well
water-Level Contour ,,..,.,,-,, (dloti.a,,,.,.,.1"•~ --Creek f Stream
□ Building I Structure
~ Inferred Direction of
""()J.1-1!5 Ground-Water Flow
7~00
.. Water level for well F-55 was
\ measured on 5/4/05
\
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-Environmental Consultants-
Figure 6. Potentiometric Surface Map
Deep Saprollte/Upper Bedrock-May 2, 2005
C."IA Holdings, Inc.lTicona
Shelby, North Carolina
-
- - - - - -- - - - - ---
850.00 A -~•:-=-=-=-=-=-=-=-=-=-=-=-~:l~•:nt'..Ar~•~•========~r=:::::::::------------11/V-astewaterTreatmentArea-----------<1
630.00
810.00
790.00
770.00
750.00
730.00
710.00
690.00
670.00
•
0-27
828.43
D-35
828.06
D-56
828.06
Legend
_5101 Line of equal fluid potential (ft msl) GJ Bedrock
(dashed ~e lllf"erred}
Potentiometric Surface Saprolite
G--50
813.93
Inferred direction of ground-water
movement
Screened Interval ofVVell
~
,----,
J-29
809.16
Horizontal Scale in Feet
0 400
'-..
"
800
' "
• C ::,
i, • ~ e a.
I
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755.53~ I GG-39
755.23
- -- -
A' 850.00
830.00
810.00
790.00
770.00
750.00
730.00
710.00
690.00
670.00
Kubal-Furr & Associates
-Environmental Consultants -
Flgure 7. Hydrogeologlc Cros..<1 Section
A-A'-:\lay 2, ZOOS
CNA Holdings, /nc.fTicoria
Shelby, North Carolina
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Attachment 1
Analytical Data Package, Data Assessment Summary and
Field Sampling Logs for the 1st and 2nd Quarter 2005 Sampling Events
-----------Kubal-Furr & Associates -----------
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DATA ASSESSMENT SUMMARY CHECKLIST AND REPORT-LEVEL II
Client ID:
Project Number:
Project Description:
Ticona, Shelby, NC
26RP21
01/05
Sample Delivery Group (SDG) Description:
Prepared By: Robert DeGaetano
Date: 07 /12/05
Seventeen aqueous samples, one field duplicate, four trip blanks and a field blank were collected
by Kubal-Furr & Associates and submitted to Davis & Floyd of Greenwood, SC for analysis.
The samples were tested for volatiles, semivolatiles, Dow Therm A parameters ( I, 1-biphenyl and
biphenyl ether) and total organic carbon. The laboratory login numbers were L0502 I 805,
L05022007, L05022303, L05022401 and L05022812. -
CONTENTS LEVEL COMMENTS
II
Sample Results ✓ Most data considered Class A as
reported. Some data are considered
Class B, and are assigned qualifiers.
Chain(s) of Custody (COCs) ✓ See Discussion
Master Tracking List ✓ Satisfactory
Method Conformance Summary ✓ Satisfactory
Batch Quality Control Report ✓ Satisfactory
Trip/Field/Equipment Blank Report ✓ Acetone detected in the field blank
Field Notes/Logbook ✓ Not reviewed
Discussion:
Acetone was detected in the field blank collected on 2/22/05 at a concentration of 0.0 I 6 mg/L.
Consequently, the acetone result for sample P-58 was flagged with a "U" qualifier. The acetone
result for K-28 (0.12 mg/L) was not qualified, however, due to the presence of this parameter
detected at the same concentration (0.12 mg/L) in March 2004. The phenol result for field
sample F-55 was flagged with a "J" qualifier due to low (<! 0%) recovery of the surrogate and
recovery values for phenol in the associated MS/MSD samples that exceeded control limits. The
reporting limits for the volatiles analysis of field samples HH-77 and F-55 were raised due to
matrix interference.
Class A = quantitative Class B = qualitative Class C = unuseable
Kubal-Furr & Associates
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DAYIS
FL6YD
April 18, 2005
PEM CARTER
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Report ID : AC1040
Page 1 of 88
LABORATORY ANALYSIS REPORT
Login Number
Project Number
Description
:L05021803, L05021805, L05022007, L05022303, L05022401,
L05022812
:61621.01
:GROUNDWATER-PROJECT #TF026QS15
Dear Pem Carter:
We are pleased to provide the enclosed analytical results for the samples received by
Davis & Floyd, Inc. on February 17, 2005 through February 24, 2005.
A formal Quality Assurance/Quality Control program is maintained by Davis & Floyd,
which is designed to meet or exceed the EPA, NELAC or other appropriate regulatory
requirements. All analytical analyses for this project met QA/QC criteria and the
results are within the 99 % confidence interval for each method unless otherwise
stated in the footnotes. This report is to be reproduced only in full.
Feel free to contact our Client Services Representative at (864) 229-4413 if further
explanation of the analysis is required. Unless other arrangements have been made,
samples will be disposed of or returned 14 days from the cfate of the report. We
appreciate the opportunity to provide services to your firm.
Sincerely, DAVI~/4INC
ohn H. McCord, Jr.
Laboratory Manager
!J;wis 8, f-loyd, Inc. I PO Drawer 42B I Greenwood, SC 29(i4c3 I 13 I h E. Durst Avenue i Creenwoorl, SC 206-1~1 I (3(,4) 22Y-4413 I Fax (8(,4) 229-71 19
DAYIS
FLtfYD
Client
Contact
LABORATORY ANALYSIS REPORT
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 2 of 88
April 18, 2005
Report ID: AC1040
Master Sample Tracking List
Sample ID
L0S0:.nso3-01
Volatile Organics
SW846 8260B
L05021803-06
Volati,10 Organics
SW846 8260B
L05021805-0l
Volatile Organics
SW846 8260B
L05021805-02
Volatile Organics
SW846 8260B
L05021805-03
Volatile Organics
SW846 8260B
L05021805-04
Volatile Organics
SW846 8260B
L05021805-05
Volatile Organics
SW846 8260B
L05021805-06
Volatile Organics
SW846 8260B
Client ID Date Collected Date Received
DUP-1
02/24/2005 0837
EB-01 02/16/2005 1351
02/24/2005 0819
HH-77
02/22/2005 1556
HH-48 02/15/2005 1354 02/17/2005
02/22/2005 1328
02/22/2005 1346
FP'-34
02/22/2005 1405
P'P-62 1705
02/22/2005 1424
GG-61 1032
02/22/2005 1442
Dcwls & Floyd, Inc. I PO Dr:1wer 428 I Creenwond, SC 2%48 I 816 E. Durst t\venue I Greenwood, SC 29649 I (864) 229-4413 I Fax (864) 229-7 l 19
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DAYIS
FLrnlD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
Master Sample Tracking List
Sample ID
L05021805-07
Volatile Organics
SW846 8260B
L0S0J:1805-08 n1n:n::~;1ni;;,r;;¥1Mw
Yolati_l'II' Organics
SW846 8260B
L05021805-09
Volatile Organics
SW846 8260B
L05021805-10
Volatile Organics
SW846 8260B
L05022007-0l
Volatile Organics
SW846 8260B
L05022007-02
l!tffil~iit#til!iiiil£i1Il
Semivolatile Organics
SW846 8270C
SW846 8270C
SW846 8270C DOWTHERM
SW846 8270C DOWTHERM
Volatile organics
SW846 8260B
L05022007-03
Volatile Organics
SW846 8260B
Client ID
AA-54
BB-58
TRIP BLANK
P-58
l"-55
CC-33
SW846 3510C
SW846 3510C
SW846 3500B
SW846 3500B
NC Cenijication Number: 25
Project Number: 61621.01
Report Date
Page 3 of 88
Date Collected
Ol/1'/2005 1033
02/03/2005 1450
Ol/18/1005 1355
02/22/2005 0800
02/22/2005 0800
02/22/2005 0800
02/22/2005 0800
April 18, 2005
Report ID: AC1040
Date Received
02/22/2005 1501
02/17/2005
02/22/2005 1519
02/17/2005
02/22/2005 1538
02/17/2005
02/24/2005 0743
02/21/2005 1544
02/11/20011
IM!U~UitRi.#.~(#\Ht:
03/01/2005 1845
03/02/2005 1256
03/01/2005 1806
03/01/2005 1845
02/21/2005 1620
02/21/2005 1602
0;1vis & Floyd, Inc. I PO Drciwcr 428 I Crcenwood, SC 291,,18 I ll 16 E. Dt1rst Avenue I Cree11wood, SC 29(i49 I (8fl4) 22:J-441 J I fax (8(,4) 22'J-7 \ ·1 ~
Dl\:YIS
FL(}YD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem carter
Master Sample Tracking List
Sample ID
L05022007-04
Volatile Organics
SW846 8260B
L05022303-0l
m::i:mn~;ifli;;1n;;@JMtm
s .. iYoi~til• Organics
SW846 827DC
SW846 8270C DOWTHERM
Volatile Organics
SW846 8260B
Semivolatile Organics
SW846 8270C
SW846 B270C DOWTHERM
SW84 6 8270C DOWTHERM
Volatile organics
SW846 8260B
L05022303-03
Semivolatile Organics
SW846 8270C
SW846 8270C DOWTHERM
Volatile Organics
SW846 8260B
LOS022303-04
Semivolatile Organics
SW846 8270C
SW846 8270C DOWTHERM
Volatile Organics
SW846 8260B
Client ID
TRIP BLANK-2
PBW-1
1Hf!fFff;;::::;;Jg;;:;
PEW-4
DUP-4
SW846 3510C
SW846 35008
SW846 3510C
SW846 3500B
SW846 3500B
SW846 3510C
SW846 35008
SW846 3510C
SW846 3500B
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 4 of 88
Date Collected
02/22/2005 1343
April 18, 2005
Report ID: AC1040
Date Received
02/21/2005 1204
02/.ll/:z00.5
!?fKlFlFfif!tit;t::Mt?; tttitthtJJtf?tffM!Xi:rtt¥Jii!Jft>r?rr::::,::·:-:
02/28/2005 0800
02/28/2005 0800
1453
02/28/2005 0800
02/28/2005 0800
02/28/2005 0800
1443
02/28/2005 0800
02/28/2005 0800
02/28/2005 0800
02/28/2005 0800
03/03/2005 1238
03/03/2005 1238
02/24/2005 0856
03/03/2005 1515
03/03/2005 1438
03/03/2005 1756
02/24/2005 0915
02/l2/2005
03/03/2005 1557
03/03/2005 1557
02/24/2005 0933
03/03/2005 1636
03/03/2005 1636
02/24/2005 0951
Dcwis & Floyd, Inc I PO Drawer 428 I Creenwood, SC 21J64B I HI G F.. Durst Avcnu~ I Cmenwood, SC 2%49 I (864) 22~-441 '.\ I F;ix (864) 229-71 t 9
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0~11s
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA, LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 2B152
Pem Carter
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page s of BB
April 18, 2005
Report ID: AC1040
Master Sample Tracking List
Sample ID
L05022303-05
Volatile Organics
SW846 8260B
L05022401-01
Client ID
TRIP BLANK-3
V-23 @t:nm:;w.i;H;~m:~u~~~at :::::::::::;:;tt:t:Jttt::=+~¥.;1:r•'.®.;~
Volatile Organics
SW846 8260B
Wet Chemistry
SW846 9060
L05022401-02
Volatile Organics
SW846 8260B
Wet Chemistry
SW846 9060
JC-28
L05022401-03 TRIP BLANK-4 :n:n:ntMARW£~@1i1M¥trn:n:n:n:n:n:n:n::n:i:,1;1r;;:~~m:
Volatile Organics
SW846 8260B
L05022812-01
Semivolatile Organics
SW846 8270C
SW846 8270C DOWTHERM
Volatile Organics
SW846 8260B
PB-01
SW846 3510C
SWB46 3500B
Date Collected
0900
02/23/2005 0945
?dttftffft/:H?t!t;;i(~~.~,id
02/22/2005 1715
02/01/200.5 0900
iiif~ji~~i~\l:li
02/22/2005 1745
02/28/2005 0800
02/28/2005 0800
Date Received
02/24/2005 0801
02/ll/2005
:n:4-~_!Y.it~t~~itt
02/24/2005 1246
03/03/2005 2002
02/24/2005 1343
03/03/2005 2027
02/23/2005 nrrrnu~ii;~nr¥.;.t:;:r
02/24/2005
02/24/2005 1227
03/03/2005 1715
03/03/2005 1715
03/03/2005 1216
Davis & Flnyd, Inc. I PO Drawer 428 I Greenwood, SC 2964H I 81 h E. Durst Avenue I Greenwood, SC 29649 I {864) 22.9-4413 I Fax (864) 219-7119
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LABORATORY ANALYSIS REPORT I
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NC Certification Number: 25
Client TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 18, 2005 I
Contact Pem Carter Page 6 of 88 Report ID: AC1040
Client ID: DUP-1 Sample ID L05021803-01
Date Collected: 02/16/2005 0000 I
Matrix GW/ChemW Date Received 02/17/2005
Parameter Result Qual RDL Units Analyst Date Time I
Volatile organics
SW846 8260B
1,1,1-TRICHLOROETHANE ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 0837 I
1,1,2,2-TETRACHLOROETHANE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0837
1,1,2-TRICHLOROETHANE ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 0837
1, 1-DICH_LOROETHANE ' o. 0010 0 .0010 mg/1 PAP 02/24/2005 0837
1 , 1-DI.CHLOROETHENE ' 0.0010 0. 0010 mg/1 PAP 02/24/2005 0837 I
1,2-DICHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0837
1,2-DICHLOROPROPANE ' 0 . 0010 0.0010 mg/1 PAP 02/24/2005 0837
2-BUTANONE ' 0. 0050 0.0050 mg/1 PAP 02/24/2005 0837
2-HEXANONE ' 0. 0050 0.0050 mg/1 PAP 02/24/2005 0837
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4-METHYL-2-PENTANONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0837
ACETONE ' 0 .0050 0.0050 mg/1 PAP 02/24/2005 0837
BENZENE ' o. 0010 0.0010 mg/1 PAP 02/24/2005 0837 I
BROMODICHLOROMETHANE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0837
BROMOFORM ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0837
BROMOMETHANE ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 0837
CARBON DISULFIDE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0837 I
CARBON TETRACHLORIDE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0837
CHLOROBENZENE ' o. 0010 0.0010 mg/1 PAP 02/24/2005 0837
CHLOROETHANE ' 0 . 0010 0.0010 mg/1 PAP 02/24/2005 0837
CHLOROFORM ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 0837 I
CHLOROMETHANE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0837
CIS-1,2-DICHLOROETHENE ' 0 . 0010 0.0010 mg/1 PAP 02/24/2005 0837
CIS-1,3-DICHLOROPROPENE ' o. 0010 0.0010 mg/1 PAP 02/24/2005 0837 I
DIBROMOCHLOROMETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0837
ETHYLBENZENE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0837
METHYLENE CHLORIDE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0837
STYRENE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0837 I
TETRACHLOROETHENE ' 0 .. 0010 0.0010 mg/1 PAP 02/24/2005 0837
TOLUENE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0837
TRANS-1,2-DICHLOROETHENE ' 0 . 0010 0.0010 mg/1 PAP 02/24/2005 0837
TRANS-1,3-DICHLOROPROPENE ' o. 0010 0 .0010 mg/1 PAP 02/24/2005 0837 I
TRICHLOROETHENE ' 0 .0010 0. 0010 mg/1 PAP 02/24/2005 0837
VINYL ACETATE ' 0.0010 0 . 0010 mg/1 PAP 02/24/2005 0837
VINYL CHLORIDE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0837 I
XYLENE (TOTAL) ' 0.0020 0.0020 mg/1 PAP 02/24/2005 0837
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Davis 81 Floyd, Inc. I PO D1awer 42H ) Greenwood, SC 2%48 I 816 I::. Durst Avenue I Greenwnod, 5C 29G4'.J I (HM) 229-4413 I f-.ix (8fi4) 22<:l-7119 I
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Dl\VIS
FLffl[D
Client
Contact
Client
Matrix
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
ID:
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLQROETHANE
1,1-DICHLOROETHANE
1,1-DLCHLOROETHENE
1,2-DICHLOROETHANE
l·, 2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
LABORATORY ANALYSIS REPORT
NC Cenijication Number: 25
TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Pem Carter Page 7 of 88 Report ID: AC1040
BB-01 Sample ID L05021803-06
Date Collected: 02/16/2005 1351
GW/Chemw Date Received 02/17/2005
Result Qual RDL Units Analyst Date Time
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0 0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0 0050 0.0050 mg/1 PAP 02/24/2005 0819
< 0.0050 0.0050 mg/1 PAP 02/24/2005 0819
< 0.0050 0.0050 mg/1 PAP 02/24/2005 0819
o. 011 0.0050 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0 0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0. 0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0 0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0 .0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0 .0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0 .0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0. 0010 0.0010 mg/1 PAP 02/24/2005 0819
< 0.0020 0.0020 mg/1 PAP 02/24/2005 0819
D3vis & Floyd, lnc. I PO Drawer 4213 I Cret:nwood, SC 2964H I 81 fi E. Durst Avenue I Greemvnod, SC 29()49 I (8G4) 229-44.U I Fax (864) 229-71 19
DAYIS
FLtrYD
Client
Contact
Client ID:
Matrix
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DIC~LOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1', 2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE.
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
LABORATORY ANALYSIS REPORT
NC Cenificarion Number: 25
TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report. Date April 18, 2005
Pem Carter Page a of 88 Report ID: AC1040
HH-77 Sample ID L05021805-01
Date Collected: 02/15/2005 1255
GW/Chemw Date Received 02/17/2005
Result Qual RDL Units Analyst Date Time
< 0.0030 X 0 . 0030 mg/1 PAP 02/22/2005 1556
< 0.0030 X 0 .0030 mg/1 PAP 02/22/2005 1556
< 0.0030 X 0 . 0030 mg/1 PAP 02/22/2005 1556
< 0.0030 X 0 .0030 mg/1 PAP 02/22/2005 1556
< 0.0030 X o. 0030 mg/1 PAP 02/22/2005 1556
< 0.0030 X 0.0030 mg/1 PAP 02/22/2005 1556
< 0.0030 X 0.0030 mg/1 PAP 02/22/2005 1556
< 0 .015 X 0 .015 mg/! PAP 02/22/2005 1556
< 0 .015 X 0 .015 mg/1 PAP 02/22/2005 1556
< 0 .015 X 0.015 mg/1 PAP 02/22/2005 1556
< 0.015 X 0.015 mg/1 PAP 02/22/2005 1556
< 0 .0030 X 0.0030 mg/1 PAP 02/22/2005 1556
< 0 .0030 X 0.0030 mg/1 PAP 02/22/2005 1556
< 0 .0030 X 0. 0030 mg/1 PAP 02/22/2005 1556
< 0. 0030 X 0 . 0030 mg/! PAP 02/22/2005 1556
< 0. 0030 X o. 0030 mg/1 PAP 02/22/2005 1556
< 0. 0030 X 0.0030 mg/! PAP 02/22/2005 1556
< 0.0030 X 0. 003 0 mg/1 PAP 02/22/2005 1556
< 0.0030 X 0. 003 0 mg/1 PAP 02/22/2005 1556
< 0.0030 X 0.0030 mg/! PAP 02/22/2005 1556
< 0 .0030 X 0.0030 mg/1 PAP 02/22/2005 1556
< 0 . 0030 X 0 . 0030 mg/1 PAP 02/22/2005 1556
< 0 . 0030 X 0 . 0030 mg/1 PAP 02/22/2005 1556
< o. 0030 X 0.0030 mg/1 PAP 02/22/2005 1556
< 0 .0030 X 0.0030 mg/1 PAP 02/22/2005 1556
< 0 .0030 X 0.0030 mg/1 PAP 02/22/2005 1556
< 0.0030 X 0. 003 0 mg/! PAP 02/22/2005 1556
< 0.0030 X 0.0030 mg/1 PAP 02/22/2005 1556
< 0.0030 X 0.0030 mg/1 PAP 02/22/2005 1556
< 0 .0030 X 0.0030 mg/1 PAP 02/22/2005 1556
< 0 .0030 X 0.0030 mg/1 PAP 02/22/2005 1556
0.38 0.0030 mg/1 PAP 02/22/2005 1556
< 0.0030 X 0.0030 mg/1 PAP 02/22/2005 1556
< 0 .0030 X 0. 003 0 mg/1 PAP 02/22/2005 1556
< 0 .0060 X 0.0060 mg/1 PAP 02/22/2005 1556
1);1vi~ & Floyd, Inc. I PO Drawer 428 I Creenwood, SC 29fi41l I !YI 6 I:. Durst Avenue I Crcenwo1Jd, SC 2%4~) I (/l64) 22Y-441] I Fax (81i4) 229-71 1 Y
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DAYIS
FLMD
Client
Contact
Client ID:
Matrix '
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1, 1-DICH,LOROETHANE
'' 1,1-DLCHLOROETHENE
1,2-DICHLOROETHANE
1·, 2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETIWIE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRA.NS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
LABORATORY ANALYSIS REPORT
NC Certification Number: 25
TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Pem Carter Page 9 of 88 Report ID: AC1040
HH-48 Sample ID L05021805-02
Date Collected: 02/15/2005 1354
GW/ChemW Date Received 02/17/2005
Result Qual RDL units Analyst Date Time
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0050 0.0050 mg/1 PAP 02/22/2005 1328
< 0.0050 0.0050 mg/1 PAP 02/22/2005 1328
< 0.0050 0.0050 mg/1 PAP 02/22/2005 1328
< 0.0050 0.0050 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/.2005 1328
< 0.0010 0.0010 mg/1 PAP 0.2/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< o. 0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 o. 0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
0.20 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1328
< 0.0010 0 . 0010 mg/1 PAP 02/22/2005 1328
< 0.0020 0. 002 0 mg/1 PAP 02/22/2005 1328
D;1vis & Fluyd, Inc. I !'0 Druwcr 42H I C1ccnwood, SC 2%4/-1 I a 16 E. lJur~t Avenue I Cn~enwood, SC 'J.9649 I (1Hi4} 229-4413 I r'ax (8fi4) 229-711 Y
DAYIS
FLbYD
Client
Contact
Client ID:
Matrix
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1, 1-DICH_LOROETHANE
1, 1-DI.CHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETI-WfE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
LABORATORY ANALYSIS REPORT
NC Certification Number: 25
TICONA,LLC Project Number; 61621. 01
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 1B, 2005
Pem Carter Page 10 of 88 Report ID: AC1040
C-49 Sample ID L05021805-03
Date Collected: 02/15/2005 1500
GW/ChemW Date Received 02/17/2005
Result Qual RDL units Analyst Date Time
' 0. 0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0 . 0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0.0010 0.0010 mg/1 PAP 02/22/2005 134 6
' 0.0010 0.0010 mg/1 PAP 02/22/2005 134 6
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0. 0050 0.0050 mg/1 PAP 02/22/2005 134 6
' 0.0050 0.0050 mg/1 PAP 02/22/2005 1346
' 0 .0050 0.0050 mg/1 PAP 02/22/2005 1346
' 0 . 0050 0.0050 mg/1 PAP 02/22/2005 1346
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0.0010 0 .0010 mg/1 PAP 02/22/2005 1346
' 0.0010 0 . 0010 mg/1 PAP 02/22/2005 134 6
' 0.0010 o. 0010 mg/1 PAP 02/22/2005 1346
' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0. 0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0 .0010 0. 0010 mg/1 PAP 02/22/2005 1346
' o. 0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0 .. 0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0.0010 0.0010 mg/1 PAP 02/22/2005 134 6
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0.0010 0. 0010 mg/1 PAP 02/22/2005 1346
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1346
' 0.0020 0. 002 0 mg/1 PAP 02/22/2005 1346
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I HHi E. Durst Avenue I Creenwood, SC 2%49 I (f.164) 229-44 U I F,1x (864) 229-7119
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DAjlS
FLOYD
Client
Contact
Client
Matrix
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
ID:
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1, 1-orCH.LOROETHENE
1,2-DICHLOROETHANE
1·, 2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
LABORATORY ANALYSIS REPORT
NC Certification Number: 25
TICONA,LLC Project Number: 61621. 01
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Pem Carter Page 11 of 88 Report ID: AC1040
FF-34 Sample ID L05021805-04
Date Collected: 02/15/2005 1619
GW/ChemW Date Received 02/17/2005
Result Qual RDL Units Analyst Date Time
< 0 .0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0 .0010 0. 0010 mg/1 PAP 02/22/2005 1405
< 0 .0010 0. 0010 mg/1 PAP 02/22/2005 1405
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0.0050 0.0050 mg/1 PAP 02/22/2005 1405
< 0.0050 0.0050 mg/1 PAP 02/22/2005 1405
< 0.0050 0.0050 mg/1 PAP 02/22/2005 1405
< 0.0050 0.0050 mg/1 PAP 02/22/2005 1405
< 0.0010 0.0010 mg/1 PAP 02/2:2/2005 1405
< 0. 0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0 0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0 0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0 .0010 0.0010 mg/1 PAP 02/22/2005 1405
< o. 0010 0.0010 mg/1 PAP 02/22/2005 1405
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0 0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0 0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0 .0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0 . 0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0. 0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1405
< 0.0020 0.0020 mg/1 PAP 02/22/2005 1405
D.ivis & r:loyd, Inc. I PO Drawer 428 j Greenwood, SC ~9648 I 816 1-:. Dur.<-t Avenu,~ I Greenwood, SC ~9649 I (864) 229-4413 I Fax (864) 229-71 I~
I
LABORATORY ANALYSIS REPORT I
I
NC Certification Number: 25
Client TICONA,LLC Project Number: 61621.01 I
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 18, 2005 I
Contact Pem Carter Page 12 of 88 Report ID: AC1040
Client ID: l"F-62 Sample ID L05021805-05
Date Collected: 02/15/:2005 1705 I
Matrix ' GW/ChemW Date Received 02/17/2005
Parameter Result Qual RDL Units Analyst Date Time I
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE ' o. 0010 0 . 0010 mg/1 PAP 02/22/2005 1424 I
1,1,2,2-TETRACHLOROETHANE ' 0 .0010 0 .0010 mg/1 PAP 02/22/2005 1424
1,1,2-TRICHLOROETHANE ' 0 .0010 0. 0010 mg/1 PAP 02/22/2005 1424
1,1-DICHLOROETJ-W.l"E ' 0 . 0010 0. 0010 mg/1 PAP 02/22/2005 1424
l,1-DICHL0ROETHENE ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1424 I
1,2-DICHLOROETHANE ' 0.0010 0 .0010 mg/1 PAP 02/22/2005 1424
1,2-DICHLOROPROPANE ' 0.0010 0. 0010 mg/1 PAP 02/22/2005 1424
2-BUTANONE ' 0 . 0050 0.0050 mg/! PAP 02/22/2005 1424
2-HEXANONE ' 0 .0050 0 .0050 mg/1 PAP 02/22/2005 1424 I
4-METHYL-2-PENTANONE ' 0 .0050 o. 0050 mg/1 PAP 02/22/2005 1424
ACETONE ' 0.0050 0.0050 mg/1 PAP 02/22/2005 1424
BENZENE . ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1424 I
BROMODICHLOROMETHANE ' 0. 0010 0.0010 mg/1 PAP 02/22/2005 1424
BROMOFORM ' o. 0010 0.0010 mg/1 PAP 02/22/2005 1424
BROMOMETHANE ' 0 .0010 0 . 0010 mg/1 PAP 02/22/2005 1424
CARBON DISULFIDE ' 0 .0010 0 .0010 mg/1 PAP 02/22/2005 1424 I
CARBON TETRACHLORIDE ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1424
CHLOROBENZENE ' o. 0010 0.0010 mg/1 PAP 02/22/2005 1424
CHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1424
CHLOROFORM ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1424 I
CHLOROMETHANE ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1424
CIS-1,2-DICHLOROETHENE ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1424
CIS-1,3-0ICHLOROPROPENE ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1424 I
DIBROMOCHLOROMETHANE ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1424
ETHYLBENZENE ' 0 .0010 0.0010 mg/! PAP 02/22/2005 1424
METHYLENE CHLORIDE ' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1424
STYRENE ' 0. 0010 0.0010 mg/1 PAP 02/22/2005 1424 I
TETRACHLOROETHENE ' 0 .0010 0 . 0010 mg/1 PAP 02/22/2005 1424
TOLUENE ' o. 0010 0 . 0010 mg/1 PAP 02/22/2005 1424
TRANS-1,2-DICHLOROETHENE ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1424
TRANS-1,3-DICHLOROPROPENE ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1424
TRICHLOROETHENE ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1424
VINYL ACETATE ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1424
VINYL CHLORIDE ' 0.0010 0.0010 mg/1 PAP 02/22/2005 1424
XYLENE (TOTAL) ' 0.0020 0.0020 mg/1 PAP 02/22/2005 1424
I
Davis 8, Floyd, Inc. I PO Orc1wer 428 I Greenwood, SC 2%413 I WI 6 t. Durst Avenue I Creenwuod, SC 29649 I (864) 22'.)-441 :l I Fax (8h4) 22'.l-7I1 '.J I
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DAYIS
FLOYD
Client
Contact
Client
Matrix
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
ID:
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DI~HLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS·l,2·DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3·DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
LABORATORY ANALYSIS REPORT
NC Cenification Number: 25
TICONA,LLC Project Number: 61621. 01
2525 BLACKSBURG ROAD
HWY 198
SHELBY. NC 28152 Report Date April 18, 2005
Pem Carter Page 13 of 88 Report ID: AC1040
GG-61 Sample ID L05021805-06
Date Collected: 02/16/2005 1032
GW/ChemW Date Received 02/17/2005
Result Qual RDL Units Analyst Date Time
< 0.0010 0 .0010 mg/1 PAP 02/22/2005 1442
< 0.0010 o. 0010 mg/1 PAP 02/22/2005 1442
< 0.0010 o. 0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0 0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0 0010 mg/1 PAP 02/22/2005 1442
< 0.0050 0 0050 mg/1 PAP 02/22/2005 1442
< 0.0050 0 0050 mg/1 PAP 02/22/2005 1442
< 0.0050 0 0050 mg/1 PAP 02/22/2005 1442
< 0.0050 0 .0050 mg/1 PAP 02/22/2005 1442
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0 0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0 0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0 0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0 0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0 . 0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1442
< o. 0010 0. 0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0 .0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0 . 0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0. 0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0 .0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0. 0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1442
< 0. 0020 0.0020 mg/1 PAP 02/22/2005 1442
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I Hl 6 E. Durst Avenue I Greenwonrl. SC 29649 I (8641 229-4413 I Fax (864) 229-71 19
DAYIS
FLtfYD
Client
Contact
Client
Matrix
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
ID:
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1, 1-DI,c°HLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLO RO ETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
LABORATORY ANALYSIS REPORT
NC Certification Number: 25
TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Pem Carter Page 14 of 88 Report ID: AC1040
T-35 Sample ID L05021805-07
Date Collected: 02/16/2005 1240
GW/ChemW Date Received 02/17/2005
Result Qual RDL Units Analyst Date Time
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1501
< 0.0010 0 .0010 mg/1 PAP 02/22/2005 1501
< 0.0010 o. 0010 mg/1 PAP 02/22/2005 1501
< 0.0010 0. 0010 mg/1 PAP 02/22/2005 1501
< 0 .0010 0.0010 mg/1 PAP 02/22/2005 1501
< 0 .0010 0.0010 mg/1 PAP 02/22/2005 1501
< 0 .0010 0.0010 mg/1 PAP 02/22/2005 1501
< 0 .0050 0.0050 mg/1 PAP 02/22/2005 1501
< 0 .0050 0.0050 mg/1 PAP 02/22/2005 1501
< 0.0050 0.0050 mg/1 PAP 02/22/2005 1501
< 0.0050 0.0050 mg/1 PAP 02/22/2005 1501
< 0.0010 0. 0010 mg/1 PAP 02/22/2005 1501
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1501
< 0.0010 0 .0010 mg/1 PAP 02/22/2005 1501
< 0.0010 0 .0010 mg/1 PAP 02/22/2005 1501
< 0.0010 0 . 0010 mg/1 PAP 02/22/2005 1501
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1501
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1501
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1501
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1501
< 0.0010 0 .0010 mg/1 PAP 02/22/2005 1501
< 0.0010 0 . 0010 mg/1 PAP 02/22/2005 1501
< 0 . 0010 o. 0010 mg/1 PAP 02/22/2005 1501
< 0 .0010 0.0010 mg/1 PAP 02/22/2005 1501
< 0. 0010 0.0010 mg/1 PAP 02/22/2005 1501
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1501
0.0010 0. 0010 ' < mg/1 PAP 02/22/2005 1501
< 0:0010 0.0010 mg/1 PAP 02/22/2005 1501
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1501
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1501
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1501
0.0016 0. 0010 mg/1 PAP 02/22/2005 1501
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1501
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1501
< 0.0020 0.0020 mg/1 PAP 02/22/2005 1501
Davis & Floyd, Inc. I PO Drawer 42H / Greenwood. SC 29648 I B 16 E. Durst Avenue I Greenwood, SC 2%49 ) (flfJ4) 229-4413 I fax (1ff,4J 229-7119
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D:\YIS
FLOYD
Client
Contact
Client
Matrix
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
ID:
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICH~ROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2 PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHE~E
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
LABORATORY ANALYSIS REPORT
NC Cenijication Number: 25
TICONA,LLC Project Number: 61621. 01
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Pem Carter Page 15 of 88 Report ID: AC1040
AA-54 Sample ID L05021BOS~OB
Date Collected: 02/16/2005 1033
GW/Chemw Date Received 02/17/2005
Result Qual RDL Units Analyst Date Time
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0 .0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0050 0.0050 mg/1 PAP 02/22/2005 1519
' 0.0050 0.0050 mg/1 PAP 02/22/2005 1519
' 0.0050 0.0050 mg/1 PAP 02/22/2005 1519
' 0.0050 0.0050 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0 0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' o._0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0 . 0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0010 0.0010 mg/1 PAP 02/22/2005 1519
' 0.0020 0. 002 0 mg/1 PAP 02/22/2005 1519
Davis & Floyd, Inc. I PO Dr<1wer 428 I Creenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, 5C 29649 I (ll(,4) 229-4413 I Fax (864) 229-7119
DAYIS FLfrYD
Client
Contact
Client
Matrix
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
ID:
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1, 1-Dr,cHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BlITANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
LABORATORY ANALYSIS REPORT
NC Certification Number: 25
TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Pem Carter Page 16 of 88 Report ID: AC1040
EB-58 Sample ID L05021805-09
Date Collected: 02/16/2005 1153
GW/ChemW Date Received 02/17/2005
Result Qual RDL Units Analyst Date Time
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0.0010 0.0010 mg/1 PAP 02/22/2005 153 8
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0. 0010 0. 0010 mg/1 PAP 02/22/2005 1538
< 0.0050 0.0050 mg/1 PAP 02/22/2005 1538
< 0.0050 0.0050 mg/1 PAP 02/22/2005 1538
< 0.0050 0.0050 mg/1 PAP 02/22/2005 1538
< 0 .0050 0.0050 mg/1 PAP 02/22/2005 153 8
< 0. 0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0 0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0 .0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0. 0010 0.0010 mg/1 PAP 02/22/2005 1538
< o. 0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0 0010 o. 0010 mg/1 PAP 02/22/2005 1538
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0.0010 0 0010 mg/1 PAP 02/22/2005 1538
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0 .0010 0.0010 mg/_1 PAP 02/22/2005 1538
< 0. 0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0. 0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0 0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0 ._0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0. 0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0. 0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0 0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0 0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0 .0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0.0010 0.0010 mg/1 PAP 02/22/2005 1538
< 0.0020 0. 002 0 mg/1 PAP 02/22/2005 1538
Davis & Floyd, Inc. I PO Druwer 428 I Greenwood. SC 2%413 I 81 (i E. Durst Avenue I Greenwood. SC 29649 I (804) 229-441 '.I I Fax (804) 229-7119
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D~IS
FLOYD
Client
Contact
Client
Matrix
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
ID:
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1, 1-DICH,LOROETHANE
1, 1-DI,CHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
LABORATORY ANALYSIS REPORT
NC Cenification Number: 25
TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Pem Carter Page 17 of BB Report ID: AC1040
TRIP BLANlC Sample ID LOS021805-10
Date Collected: 02/03/2005 1450
GW/Chemw Date Received 02/17/2005
Result Qual RDL Units Analyst Date Time
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0 .0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0050 0.0050 mg/1 PAP 02/24/2005 0743
' 0.0050 0.0050 mg/1 PAP 02/24/2005 0743
' 0.0050 0.0050 mg/1 PAP 02/24/2005 0743
' 0.0050 0.0050 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0. 0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0. 0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0: 0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0. 0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0 . 0010 0.0010 mg/1 PAP 02/24/2005 0743
' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0743
' o. 0020 0.0020 mg/1 PAP 02/24/2005 0743
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood. SC 29648 I 816 E. Durst Avenue I Greenwood, SC 2%49 I (8(l4) :229-4413 ] Fax (864) 229-7119
I
LABORATORY ANALYSIS REPORT I
I
NC Certijica1ion Number: 25
I Client TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 18, 2005 I
Contact Pem Carter Page 18 of 88 Report ID: AC1040
Client ID: P-58 Sample ID L05022007-01
Date collected: 02/17/2005 1820 I
Matrix GW/ChemW Date Received 02/18/2005
Parameter Result Qual RDL Units Analyst Date Time I
Volatile Organ_ics
SW846 8260B
1,1,1-TRICHLOROETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544 I
1,1,2,2-TETRACHLOROETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544
1,1,2-TRICHLOROETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544
1,1-DICHLOROETHANE < 0. 0010 0.0010 mg/1 PAP 02/21/2005 1544
1, 1-DI,CHLOROETHENE < 0. 0010 0.0010 mg/1 PAP 02/21/2005 1544 I
1,2-DICHLOROETHANE < 0.0010 0 .0010 mg/1 PAP 02/21/2005 1544
1,2-DICHLOROPROPANE < 0.0010 0 . 0010 mg/1 PAP 02/21/2 DOS 1544
2-BUTANONE < 0.0050 o.ooso mg/1 PAP 02/21/2005 1544 I 2-HEXANONE < 0.0050 0.0050 mg/1 PAP 02/21/2005 1544
4-METHYL-2-PENTANONE < 0.0050 0.0050 mg/1 PAP 02/21/2005 1544
ACETONE 0.0091 0.0050 mg/1 PAP 02/21/2005 1544
BENZENE < o. 0010 0.0010 mg/1 PAP 02/21/2005 1544 I
BROMODICHLOROMETHANE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1544
BROMOFORM < 0. 0010 0.0010 mg/1 PAP 02/21/2005 1544
BROMOMETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544
CARBON DISULFIDE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544 I
CARBON TETRACHLORIDE < 0.0010 0. 0010 mg/1 PAP 02/21/200S 1S44
CHLOROBENZENE < o. 0010 0. 0010 mg/1 PAP 02/21/2005 1544
CHLOROETHANE < o. 0010 0.0010 mg/1 PAP 02/21/2005 1544
CHLOROFORM < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544 I
CHLOROMETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544
CIS-1,2-DICHLOROETHENE < 0. 0010 0.0010 mg/1 PAP 02/21/2005 1544
CIS-1,3-DICHLOROPROPENE < 0. 0010 0. 0010 mg/1 PAP 02/21/200S 1544 I
OIBROMOCHLOROMETHANE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1544
ETHYLBENZENE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544
METHYLENE CHLORIDE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544
STYRENE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544 I
TETRACHLOROETHENE < 0:0010 0.0010 mg/1 PAP 02/21/2005 1544
TOLUENE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1544
TRANS-1,2-DICHLOROETHENE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1544
TRANS-1,3-DICHLOROPROPENE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1544 I
TRICHLOROETHENE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1544
VINYL ACETATE < 0 . 0010 0.0010 mg/1 PAP 02/21/2005 1544
VINYL CHLORIDE < 0 . 0010 0.0010 mg/1 PAP 02/21/2005 1544 I
XYLENE {TOTAL) < 0 .0020 0.0020 mg/1 PAP 02/21/2005 1544
I
D;wis & Floyd, Inc. I PO Dr<1wer 428 I Creenwood, SC 29648 I 81 fi E. Durst Avenue I Greenwood, SC 29649 I (864) 229-4413 I F.Jx (f\64) 229-71 19 I
I
I D~IS FL ~YD LABORATORY ANALYSIS REPORT
I
NC Cenification Number: 25
I Client TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
I HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Contact Fem Carter Page 19 of 88 Report ID: AC1040
I Client ID: l'-55 sample ID L05022007-02
Date Collected: 02/18/2005 1355
Matrix GW/ChemW Date Received 02/18/2005
I Parameter Result Qual RDL Units Analyst Date Time
Semi volatile Organics
I SW845 8270C
1,2,4-TRICHLOROBENZENE < 0.010 o. 010 mg/1 JRN 03/01/2005 1845
1,2-DICHLOROBENZENE < 0.010 o. 010 mg/1 JRN 03/01/2005 1845
I 1,3-DICHLOROBENZENE < 0.010 0 .010 mg/1 JRN 03/01/2005 1845
1,4-DICHµJROBENZENE < 0.010 0.010 mg/1 JRN 03/01/2005 1845
2, 4, 5-.TRICHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/01/2005 1845
2,4,6-TRICHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/01/2005 1845
I 2,4-DICHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/01/2005 1845
2,4-DIMETHYLPHENOL < 0.010 0.010 mg/1 JRN 03/01/2005 1845
2,4-DINITROPHENOL < 0.025 0.025 mg/1 JRN 03/01/2005 1845
2,4-DINITROTOLUENE < 0.010 0.010 mg/1 JRN 03/01/2005 1845
I 2,6-DINITROTOLUENE < 0. 010 0.010 mg/1 JRN 03/01/2005 1845
2-CHLORONAPHTHALENE < 0.010 0.010 mg/1 JRN 03/01/2005 1845
2 -CHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/01/2005 1845
I 2-METHYL-4,6-DINITROPHENOL < 0.025 0.025 mg/1 JRN 03/01/2005 1845
2-METHYLNAPHTHALENE 0.074 0.010 mg/1 JRN 03/01/2005 1845
2-METHYLPHENOL < 0.010 0.010 mg/1 JRN 03/01/2005 1845
2-NITROANILINE < 0.010 0.010 mg/1 JRN 03/01/2005 1845
I 2-NITROPHENOL < 0 010 0.010 mg/1 JRN 03/01/2005 1845
3,3'-DICHLOROBENZIDINE < 0.010 0.010 mg/1 JRN 03/01/2005 1845
3-NITROANILINE < 0.010 0.010 mg/1 JRN 03/01/2005 1845
4-BROMOPHENYL PHENYL ETHER < 0.010 0.010 mg/1 JRN 03/01/2005 1845
I 4-CHLOR0-3-METHYLPHENOL < 0.010 0.010 mg/1 JRN 03/01/2005 1845
4 -CHLOROANI LINE < 0.010 0.010 mg/1 JRN 03/01/2005 1845
4-CHLOROPHENYL PHENYL ETHER < 0.010 0.010 mg/1 JRN 03/01/2005 1845
I 4-METHYLPHENOL < 0.010 0.010 mg/1 JRN 03/01/2005 1845
4-NITROANILINE < 0.010 0.010 mg/1 JRN 03/01/2005 1845
4-NITROPHENOL < 0.025 0. 025 mg/1 JRN 03/01/2005 1845
ACENAPHTHENE < ().010 0.010 mg/1 JRN 03/01/2005 1845
I ACENAPHTHYLENE < 0.010 0.010 mg/1 JRN 03/01/2005 1845
ANTHRACENE < 0.010 0.010 mg/1 JRN 03/01/2005 1845
BENZO(A)ANTHRACENE < 0.010 0.010 mg/1 JRN 03/01/2005 1845
BENZO(A)PYRENE < 0. 010 0.010 mg/1 JRN 03/01/2005 1845
I BENZO(B)FLUORANTHENE < 0.010 0.010 mg/1 JRN 03/01/2005 1845
BENZO(G,H,I)PERYLENE < 0.010 0.010 mg/1 JRN 03/01/2005 1845
BENZO(K)FLUORANTHENE < 0.010 0. 010 mg/1 JRN 03/01/2005 1845
BENZOIC ACID < 0.050 0.050 mg/1 JRN 03/01/2005 1845 I BENZYL ALCOHOL < 0. 010 0. 010 mg/1 JRN 03/01/2005 1845
BIS(2-CHLOROETH0XY)METHANE < 0.010 0. 010 mg/1 JRN 03/01/2005 1845
BIS(2-CHLOROETHYL)ETHER < o. 010 0.010 mg/1 JRN 03/01/2005 1845
I BIS(2-CHLOROISOPROPYL)ETHER < 0.010 0.010 mg/1 JRN 03/01/2005 1845
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2964H I s 10 E. Durst Avenue I Creenwood. SC 29649 I (86-1) 229-4413 I Fax (864) 229-7119
I
011s I
FL '"'YD LABORATORY ANALYSIS REPORT
I
NC Cenijication Number: 25
Client TICONA,LLC Project Number, I 61621.01
2525 BLACKSBURG ROAD
HWY 198 I I SHELBY, NC 28152 Report Date April 18, 2005
Contact Pem Carter Page 20 of 88 Report ID: AC1040
Client ID: F-55 Sample ID L05022007-02 I Date Collected: 02/18/2005 1355
Matrix GW/ChemW Date Received 02/18/2005
Parameter Result Qual RDL units Analyst Date Time I
BIS(2-ETHYLHEXYL)PHTHALATE ' 0.010 0.010 mg/1 JRN 03/01/2005 1845
BUTYL BENZYL PHTHALATE ' 0. 010 0.010 mg/1 JRN 03/01/2005 1845 I CHRYSENE ' 0 .010 0.010 mg/1 JRN 03/01/2005 1845
DI -N-BUTYL PHTHALATE ' 0 .010 0.010 mg/1 JRN 03/01/2005 1845
DI-N-OCTYL PHTHALATE ' 0 .010 0.010 mg/1 JRN 03/01/2005 1845 I DIBENZ{A,H)ANTHRACENE ' 0 .010 0. 010 mg/1 JRN OJ/01/2005 1845
DIBENZOFURAN 0. 027 0.010 mg/1 JRN 03/01/2005 1845
DIETHYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/01/2005 1845
DIMETHYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/01/2005 1845 I FLUORANTHENE ' 0.010 0 .010 mg/1 JRN 03/01/2005 1845
FLUORENE ' 0.010 0 .010 mg/1 JRN 03/01/2005 1845
HEXACHLOROBENZENE ' 0.010 0 .010 mg/1 JRN 03/01/2005 1845
HEXACHLOROBUTADIENE ' 0.010 0 .010 mg/1 JRN 03/01/2005 1845 I HEXACHLOROCYCLOPENTADIENE ' 0.010 0. 010 mg/1 JRN 03/01/2005 1845
HEXACHLOROETHANE ' 0.010 O. 010 mg/1 JRN 03/01/2005 184 5
INDENO(l,2,3-CD)PYRENE ' 0.010 0 .010 mg/1 JRN 03/01/2005 1845 I ISOPHORONE ' 0.010 0 .010 mg/1 JRN 03/01/2005 1845
N-NITROSODI-N-PROPYLAMINE ' 0.010 0 .010 mg/1 JRN 03/01/2005 1845
N-NITROSOOIPHENYLAMINE ' 0.010 0. 010 mg/1 JRN 03/01/2005 184 5
NAPHTHALENE ' 0.010 o. 010 mg/1 JRN 03/01/2005 1845 I NITROBENZENE ' 0 .010 0 .010 mg/1 JRN 03/01/2005 1845
PENTACHLOROPHENOL ' 0 .025 0.025 mg/1 JRN 03/01/2005 1845
PHENANTHRENE ' 0 .010 0.010 mg/1 JRN 03/01/2005 1845
PHENOL 0.26 0.10 mg/1 JRN 03/02/2005 1256 I PYRENE ' 0.010 0.010 mg/1 JRN 03/01/2005 1845
SW846 8270C DOWTHERM
1, l' -Bl PHENYL 20.8 10.0 mg/1 JRN 03/01/2005 1806 I BIPHENYL ETHER 62.7 10.0 mg/1 JRN 03/01/2005 1806
Volatile Organics
SW846 8260B I 1,1,1-TRICHLOROETHANE ' 0 .0030 X 0.0030 mg/1 PAP 02/21/2005 162 0
1,1,2,2-TETRACHLOROETHANE ' 0 .0030 X 0 . 0030 mg/1 PAP 02/21/2005 1620
1,1,2-TRICHLOROETHANE ' 0 .0030 X 0 .0030 mg/1 PAP 02/21/2005 1620
1,1-DICHLOROETIWfE ' 0.0030 X 0 .0030 mg/1 PAP 02/21/2005 1620 I 1,1-DICHLOROETHENE ' 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620
1,2-DICHLOROETHANE ' 0 .0030 X 0.0030 mg/1 PAP 02/21/2005 1620
1,2-DICHLOROPROPANE ' o. 0030 X 0.0030 mg/1 PAP 02/21/2005 1620 I 2-BUTANONE ' 0.015 X 0.015 mg/1 PAP 02/21/2005 1620
2-HEXANONE ' 0.015 X 0.015 mg/1 PAP 02/21/2005 1620
4-METHYL-2-PENTANONE ' 0 .015 X 0 .015 mg/1 PAP 02/21/2005 1620
ACETONE ' 0 .015 X 0 .015 mg/1 PAP 02/21/2005 1620 I D;ivi~ & Floyrl, Inc. I PO Drawer 428 I Creenwoorl, SC 2%48 I s Ir, E. Durst Avenue I Greenwood, SC 2964~! / (8(i4) 229-4413 I Fax (HCi4) n9-7 t 19
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DAYIS
FLOYD
Client
Contact
Client
Matrix
Parameter
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOR0}3ENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
ID:
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Prep Procedure
Analytical Prep Procedures1
OOWTHERM
8270 SVOC PREP
LABORATORY ANALYSIS REPORT
NC Cenificarion Number: 25
TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Pem Carter Page 21 of 88 Report ID: AC1040
F-55 Sample ID L05022007-02
Date Collected: 02/18/2005 1355
GW/ChemW Date Received 02/18/2005
Result Qual RDL Units Analyst Date Time
0.051 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0 0030 X 0.0030 mg/1 PAP 02/21/2005 1620
< o. 0030 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0. 0030 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620
0. 014 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620
0.0057 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0 0030 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0.0030 X 0.0030 mg/1 PAP 02/21/2005 1620
< 0.0030 X 0 . 0030 mg/1 PAP 02/21/2005 1620
< 0.0060 X 0.0060 mg/1 PAP 02/21/2005 1620
Method Analyst Prep Date
SWB46 3500B DBC 02/22/2005 0B00
SWB46 3510C DBC 02/22/2005 0B00
Davis & Floyd. Inc. I PO Drawer 428 I Creemvood, SC 29648 I H 16 E. Durst Avenue I Greenwood. SC 2%49 I (864) 2.29-4413 I Fax (864) n9-7119
DAYIS
FLtrYD LABORATORY ANALYSIS REPORT
NC Certification Number: 25
Client TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Contact Pem Carter Page 22 of 88 Report ID: AC1040
Client ID: CC-33 Sample ID L05022007-03
Date Collected: 02/18/2005 1019
Matrix : GW/Chemw Date Received 02/18/2005
Parameter Result Qual RDL Units Analyst Date Time
Volatile Organics
SW845 8260B
1,1,1-TRICHLOROETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602
1,1,2,2-TETRACHLOROETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602
1,1,2-TRICHLOROETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602
1, 1-DICHLOROETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602
1, 1-DI,CHLOROETHENE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602
1,2-DICHLOROETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602
1,2-DICHLOROPROPANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602
2-BUTANONE < 0.0050 0.0050 mg/1 PAP 02/21/2005 1602
2-HEXANONE < 0.0050 0.0050 mg/1 PAP 02/21/2005 1602
4-METHYL-2-PENTANONE < o.ooso 0.0050 mg/1 PAP 02/21/2005 1602
ACETONE < 0.0050 0.0050 mg/1 PAP 02/21/2005 1602
BENZENE < 0 0010 0.0010 mg/1 PAP 02/21/2005 1602
BROMODICHLOROMETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602
BROMOFORM < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602
BROMOMETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602
CARBON DISULFIDE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602
CARBON TETRACHLORIDE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602
CHLOROBENZENE 0.0019 0.0010 mg/1 PAP 02/21/2005 1602
CHLOROETHANE < o. 0010 0.0010 mg/1 PAP 02/21/2005 1602
CHLOROFORM < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602
CHLOROMETHANE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602
CIS-1,2-DICHLOROETHENE 0.0022 0.0010 mg/1 PAP 02/21/2005 1602
CIS-1,3-DICHLOROPROPENE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1602
DIBROMOCHLOROMETHANE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1602
ETHYLBENZENE < 0 0010 0.0010 mg/1 PAP 02/21/2005 1602
METHYLENE CHLORIDE < 0 0010 0.0010 mg/1 PAP 02/21/2005 1602
STYRENE < 0.0010 0.0010 mg/1 PAP 02/21/2005 1602
TETRACHLOROETHENE < 0:0010 0. 0010 mg/1 PAP 02/21/2005 1602
TOLUENE < 0 . 0010 0.0010 mg/1 PAP 02/21/2005 1602
TRANS-1,2-DICHLOROETHENE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1602
TRANS-1,3-DICHLOROPROPENE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1602
TRICHLOROETHENE < 0 0010 0.0010 mg/1 PAP 02/21/2005 1602
VINYL ACETATE < 0 .0010 0.0010 mg/1 PAP 02/21/2005 1602
VINYL CHLORIDE < 0 0010 o. 0010 mg/1 PAP 02/21/2005 1602
XYLENE {TOTAL) < 0 .0020 0.0020 mg/1 PAP 02/21/2005 1602
Davis & Floyd, Inc. 1 · PO Drawer ..t28 I Greenwood, SC 29648 I 816 E. Durst Avenue / Greenwood, SC ~9649 I (864) 229-4413 I Fax (1:164) 229-71 l 9
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D~IS
FLOYD
Client
Contact
Client
Matrix
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
ID:
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
l, l-□r.cin.oROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
LABORATORY ANALYSIS REPORT
NC Certification Number: 25
TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Fem carter Page 23 of 88 Report ID: AC1040
TRIP BLANX-2 Sample ID L05022007-04
Date Collected: 02/03/2005 1450
GW/Chemw Date Received 02/18/2005
Result Qual RDL Units Analyst Date Time
< 0 0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0. 0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0 0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0 0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0 0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0.0010 0.0010 . mg/1 PAP 02/21/2005 1204
< 0.0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0 0050 0.0050 mg/1 PAP 02/21/2005 1204
< 0 .0050 0.0050 mg/1 PAP 02/21/2005 1204
< 0 .0050 0.0050 mg/1 PAP 02/21/2005 1204
< 0 0050 0.0050 mg/1 PAP 02/21/2005 1204
< 0 0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0. 0010 0.0010 mg/1 PAP 02/21/2005 1204
< o. 0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0.0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0 0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0 0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0 0010 0 0010 mg/1 PAP 02/21/2005 1204
< 0 .0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0 0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0 .0010 0. ◊-010 mg/1 PAP 02/21/2005 1204
< 0.0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0 0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0.0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0.0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0.0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0.0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0.0010 · 0.0010 mg/1 PAP 02/21/2005 1204
< 0 0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0.0010 0 .0010 mg/1 PAP 02/21/2005 1204
< 0.0010 0.0010 mg/1 PAP 02/21/2005 12 04
< 0.0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0.0010 0.0010 mg/1 PAP 02/21/2005 1204
< 0.0010 0 0010 mg/1 PAP 02/21/2005 1204
< 0.0020 0.0020 mg/1 PAP 02/21/2005 1204
D.ivis K Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC ~9649 I (864) 229-4413 I Fax (864) 229-7119
I
011s I FL ~~YD LABORATORY ANALYSIS REPORT
I
NC Certification Number: 25
Client TICONA,LLC Project Number:
I
61621.01
2525 BLACKSBURG ROAD
HWY 198 I SHELBY, NC 28152 Report Date April 18, 2005
Contact Pem Carter Page 24 of 88 Report ID: AC1040
Client ID: PEW-1 Sample ID L05022303-01 I Date Collected: 02/22/2005 1343
Matrix GW/ChemW Date Received 02/22/2005
Para.meter Result Qual RDL Units Analyst Date Time I
Semi volatile Organics
SW846 8270C I 1,2,4-TRICHLOROBENZENE < 0.010 0. 010 mg/1 JRN 03/03/2005 1238
1,2-DICHLOROBENZENE < 0.010 0.010 mg/1 JRN 03/03/2005 1238
1,3-DICHLOROBENZENE < 0.010 0. 010 mg/1 JRN 03/03/2005 1238 I 1,4-DICHLOROBENZENE < 0.010 0. 010 mg/1 JRN 03/03/2005 1238
2,4,S~TRICHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1238
2,4,6-TRICHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1238
2,4-DICHLOROPHENOL < 0 010 0.010 mg/1 JRN 03/03/2005 1238 I 2,4-DIMETHYLPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1238
2,4-DINITROPHENOL < 0 .025 0.025 mg/1 JRN 03/03/2005 1238
2,4-DINITROTOLUENE < o. 010 0.010 mg/1 JRN 03/03/2005 123 8
2,6-DINITROTOLUENE < 0. 010 0.010 mg/1 JRN 03/03/2005 1238 I 2 -CHLORONAPHTHALENE < 0.010 0. 010 mg/1 JRN 03/03/2005 1238
2 -CHLOROPHENOL < 0.010 0. 010 mg/1 JRN 03/03/2005 1238
2-METHYL-4,6-DINITROPHENOL < 0.025 0. 025 mg/1 JRN 03/03/2005 1238 I 2-METHYLNAPHTHALENE < 0. 010 0. 010 mg/1 JRN 03/03/2005 1238
2-METHYLPHENOL < 0. 010 0. 010 mg/1 JRN 03/03/2005 1238
2-NITROANILINE < 0.010 0 010 mg/1 JRN 03/03/2005 1238
2-NITROPHENOL < 0.010 0 010 mg/1 JRN 03/03/2005 1238 I 3,3'-DICHLOROBENZIDINE < 0 010 0.010 mg/1 JRN 03/03/2005 1238
3-NITROANILINE < 0.010 0. 010 mg/1 JRN 03/03/2005 1238
4-BROMOPHENYL PHENYL ETHER < o. 010 0.010 mg/1 JRN 03/03/2005 123 8
4-CHLOR0-3-METHYLPHENOL < o. 010 0.010 mg/1 JRN 03/03/2005 1238 I 4-CHLOROANILINE < 0 010 0.010 mg/1 JRN 03/03/2005 1238
4-CHLOROPHENYL PHENYL ETHER < 0 010 0.010 mg/1 JRN 03/03/2005 1238
4-METHYLPHENOL < 0 010 0.010 mg/1 JRN 03/03/2005 1238 I 4-NITROANILINE < o. 010 0.010 mg/1 JRN 03/03/2005 1238
4-NITROPHENOL < 0.025 0.025 mg/1 JRN 03/03/2005 1238
ACENAPHTHENE < 0.010 0. 010 mg/1 JRN 03/03/2005 1238
ACENAPHTHYLENE < 0.010 0.010 mg/1 JRN 03/03/2005 1238 I ANTHRACENE < 0 010 0.010 mg/1 JRN 03/03/2005 1238
BENZO(A)ANTHRACENE < 0 010 0. 010 mg/1 JRN 03/03/2005 1238
BENZO(A)PYRENE < 0. 010 0.010 mg/1 JRN 03/03/2005 1238
BENZO(B)FLUORANTHENE < 0.010 0.010 mg/1 JRN 03/03/2005 1238 I BENZO(G,H,I)PERYLENE < 0.010 0.010 mg/1 JRN 03/03/2005 1238
BENZO(K)FLUORANTHENE < 0.010 0.010 mg/1 JRN 03/03/2005 1238
BENZOIC ACID < 0.050 0 .050 mg/1 JRN 03/03/2005 1238 I BENZYL ALCOHOL < 0.010 0 .010 mg/1 JRN 03/03/2005 1238
BIS(2-CHLOROETHOXY)METHANE < 0.010 0. 010 mg/1 JRN 03/03/2005 1238
BIS(2-CHLOROETHYL)ETHER < 0. 010 0.010 mg/1 JRN 03/03/2005 1238
BIS(2-CHLOROISOPROPYL)ETHER < 0.010 0 010 mg/1 JRN 03/03/2005 1238 I Davis & Floyd, Inc. I PO Drawer 428 I Greemvoud, SC 2964R I 816 E. Durst Avenue ! Creenwood, SC 29649 I (864) 229-4413 I Fax (8()4) 229-71 I~
I
I D~IS
LABORATORY ANALYSIS REPORT FLMD I
NC Cenification Number: 25
I Client TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
I HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Contact Pem Carter Page 25 of 88 Report ID: AC1040
I Client ID: PBW-1 Sample ID L05022303-01
Date Collected: 02/22/2005 1343
Matrix GW/ChemW Date Received 02/22/2005
I Parameter Result Qual RDL units Analyst Date Time
BIS(2-ETHYLHEXYL)PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238 I BUTYL BENZYL PHTHALATE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1238
CHRYSENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238
DI-N-BUTYL PHTHALATE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1238
DI-N-OCTYL PHTHALATE ' 0. 010 0. 010 mg/1 JRN 03/03/2005 1238 I DIBENZ{A,H)ANTHRACENE ' 0.010 0 010 mg/1 JRN 03/03/2005 1238
DIBEN2;0FURAN ' 0.010 0 .010 mg/1 JRN 03/03/2005 1238
DIETHYL PHTHALATE ' 0. 010 0.010 mg/1 JRN 03/03/2005 1238
I DIMETHYL PHTHALATE ' 0. 010 0.010 mg/1 JRN 03/03/2005 1238
FLUORANTHENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238
FLUORENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1238
HEXACHLOROBENZENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238
I HEXACHLOROBUTADIENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238
HEXACHLOROCYCLOPENTADIENE ' 0. 010 0. 010 mg/1 JRN 03/03/2005 1238
HEXACHLOROETHANE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238
INDENO(l,2,3-CD)PYRENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238 I ISOPHORONE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238
N-NITROSODI-N-PROPYLAMINE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238
N-NITROSODIPHENYLAMINE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238
I NAPHTHALENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238
NITROBENZENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238
PENTACHLOROPHENOL ' 0.025 0. 025 mg/1 JRN 03/03/2005 1238
PHENANTHRENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1238
I PHENOL ' 0.010 0.010 mg/1 JRN 03/03/2005 1238
PYRENE ' 0 .010 0.010 mg/1 JRN 03/03/2005 1238
SW846 8270C DOWTHERM
1, l' -BI PHENYL ' 0 010 0.010 mg/1 JRN 03/03/2005 1238 I BIPHENYL ETHER ' 0 .010 0.010 mg/1 JRN 03/03/2005 1238
Volatile Organics
I SWB46 8260B
1,1,1-TRICHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0856
1,1,2,2-TETRACHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0856
1,1,2-TRICHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0856 I 1,1-DICHLOROETHANE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0856
1,1-DICHLOROETHENE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0856
1,2-DICHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0856
1,2-DICHLOROPROPANE ' 0.0010 0. 0010 mg/1 PAP 02/24/2005 0856 I 2-BUTANONE ' o.ooso 0.0050 mg/1 PAP 02/24/2005 0856
2-HEXANONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0856
4-METHYL-2 PENTANONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0856
I ACETONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0856
Duvis & Floyd, Inc. I PO Drawer 428 I Greenwood. SC 296413 I 816 E. Durst Avenue I Creenwood, SC 29649 I (864) 229-4413 I Fa, (8641229-7119
DAYIS
FLbYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
Client ID: PEW-l
Matrix
Parlllrleter
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLORO_BENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Prep Procedure
Analytical Prep Proceduresi
OOWTHERM
8270 SVOC PREP
GW/ChemW
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
Method
SW846 3500B
SW846 3510C
Result Qual
0. 0010
0 .0010
0 .0010
0 .0010
0.0010
0.0010
0.0010
0.0010
0.0016
0.0010
0.0012.
0.0010
0.0010
0 .0010
0. 0010
0.0010
0.0010
0 . 0010
o. 0010
0 .0010
0.0055
0.0010
0.0010
0.0020
Analyst
DBC
DBC
NC Cenification Number: 25
Project Number: 61621.01
Report Date
Page 26 of 8B
April 18, 2005
Report ID: AC1040
Sample ID L05022303-01
Date Collected: 02/22/2005 1343
Date Received 02/22/2005
RDL Units
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0 . 0010 mg/1
o . 0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0. 002 0 mg/1
Prep Date
02/28/2005 0800
02/28/2005 0800
Analyst
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
Date
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
Time
0856
0856
0856
0856
0856
0856
0856
0856
0856
0856
0856
0856
0856
0856
0856
0856
0856
0856
0856
0856
0856
0856
0856
0856
D,ivis & Floyrl, Inc. / PO Drawer 428 I Greenwood, SC 2%48 I 816 E. Durst Avenue I Greenwood, SC 29649 I (H64) 229-4413 I Fax (864) 229-7119
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I D~S LABORATORY ANALYSIS REPORT FL D I
NC Certification Number: 25
I Client TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
I HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Contact Pem Carter Page 27 of 88 Report ID: AC1040
I Client ID: PEW-3 Sample ID L05022303-02
Date Collected: 02/22/2005 1453
Matrix GW/ChemW Date Received 02/22/2005
I Parameter Result Qual RDL Units Analyst Date Time
Semi volatile Organics
I SWB46 8270C
1,2,4-TRICHLOROBENZENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1515
1,2-DICHLOROBENZENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1515
1,3-DICHLOROBENZENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1515 I 1,4-DICHLOROBENZENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1515
2, 4, 5-,TRICHLOROPHENOL ' 0.010 0.010 mg/1 JRN 03/03/2005 1515
2,4,6-TRICHLOROPHENOL ' 0.010 0.010 mg/1 JRN 03/03/2005 1515
I 2,4-DICHLOROPHENOL ' 0.010 0. 010 mg/1 JRN 03/03/2005 1515
2,4-DIMETHYLPHENOL ' 0.010 0.010 mg/1 JRN 03/03/2005 1515
2,4-DINITROPHENOL ' 0. 025 0.025 mg/1 JRN 03/03/2005 1515
2,4-DINITROTOLUENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1515
I 2,6-DINITROTOLUENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1515
2-CHLORONAPHTHALENE ' 0. 010 0.010 mg/1 JRN 03/03/2005 1515
2-CHLOROPHENOL ' 0.010 0.010 mg/1 JRN 03/03/2005 1515
2-METHYL-4,6-DINITROPHENOL ' 0. 025 0.025 mg/1 JRN 03/03/2005 1515 I 2-METHYLNAPHTHALENE ' o. 010 0.010 mg/1 JRN 03/03/2005 1515
2 -METHYLPHENOL ' 0 .010 0.010 mg/1 JRN 03/03/2005 1515
2-NITROANILINE ' 0.010 0.010 mg/1 JRN 03/03/2005 1515
I 2-NITROPHENOL ' 0 010 0.010 mg/1 JRN 03/03/2005 1515
3,3'-DICHLOROBENZIDINE ' 0. 010 0.010 mg/1 JRN 03/03/2005 1515
3-NITROANILINE ' 0. 010 0.010 mg/1 JRN 03/03/2005 1515
4-BROMOPHENYL PHENYL ETHER ' 0. 010 0.010 mg/1 JRN 03/03/2005 1515
I 4-CHLOR0-3-METHYLPHENOL ' 0 .010 0. 010 mg/1 JRN 03/03/2005 1515
4-CHLOROANILINE ' 0 010 0.010 mg/1 JRN 03/03/2005 1515
4-CHLOROPHENYL PHENYL ETHER ' 0.010 0.010 mg/1 JRN 03/03/2005 1515
4-METHYLPHENOL ' 0. 010 0 .010 mg/1 JRN 03/03/2005 1515 I 4-NITROANILINE ' 0. 010 0.010 mg/1 JRN 03/03/2005 1515
4-NITROPHENOL ' 0 .025 0.025 mg/1 JRN 03/03/2005 1515
ACENAPHTHENE ' 0. 010 0.010 mg/1 JRN 03/03/2005 1515
I ACENAPHTHYLENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1515
ANTHRACENE ' 0 010 0.010 mg/1 JRN 03/03/2005 1515
BENZO(A)ANTHRACENE ' 0 010 0.010 mg/1 JRN 03/03/2005 1515
BENZO (A) PYRENE ' 0.010 0.010 mg/1 JRN 03/03/2005 15_15
I BENZO(B)FLUORANTHENE ' 0 010 0.010 mg/1 JRN 03/03/2005 1515
BENZO(G,H,I)PERYLENE ' 0 .010 0.010 mg/1 JRN 03/03/2005 1515
BENZO(K)FLUORANTHENE ' 0 010 0. 010 mg/1 JRN 03/03/2005 1515
BENZOIC ACID ' 0. 050 o.oso mg/1 JRN 03/03/2005 1515
I BENZYL ALCOHOL ' 0 010 0. 010 mg/1 JRN 03/03/2005 1515
BIS(2-CHLOROETHOXY)METHANE ' 0 010 0.010 mg/1 JRN 03/03/2005 1515
BIS(2-CHLOROETHYL)ETHER ' 0.010 0.010 mg/1 JRN 03/03/2005 1515
I 8IS(2-CHLOROISOPROPYL)ETHER ' 0.010 0.010 mg/1 JRN 03/03/2005 1515
D.ivis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue l Greenwood, SC 29649 I (BG4) 229-44 U I Fax (864) 229-711 Y
DAVIS
FL6YD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
Client ID: PEW-3
Matrix
Para.meter
BIS(2-ETHYLHEXYL)PHTHALATE
BUTYL BENZYL PHTHALATE
CHRYSENE
DI·N-BUTYL PHTHALATE
DI-N-OCTYL PHTHALATE
DIBENZ(A,H)ANTHRACENE
DIBENZOFURAN
DIETHYL PHTHALATE
DIMETHYL PHTHALATE
FLUORANTHENE
FLUORENE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROCYCLOPENTADIENE
HEXACHLOROETHANE
INDENO(l,2,3-CD)PYRENE
ISOPHORONE
N-NITROSODI-N-PROPYLAMINE
N-NITROSODIPHENYLAMINE
NAPHTHALENE
NITROBENZENE
PENTACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRENE
SW846 8270C DOWTHERM
1, 1' -BI PHENYL
BIPHENYL ETHER
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
GW/ChemW
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
Result Qual
0.010
o. 010
0 .010
0 .010
0. 010
0.010
0. 010
0.010
0. 010
0.010
0.010
0.010
0.010
0. 010
0.010
0.010
0.010
0.010
0.010
0.010
0.010
0. 025
0. 010
0. 010
0.010
0.27
0.86
0.0010
0.0010
0.0010
0.0010
0 .0010
0 .0010
0.0010
0.0050
o.ooso
0.0050
0.0050
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 28 of 88
Sample ID
Date Collected:
Date Received
RDL Units
0.010 mg/1
0.010 mg/1
0 .010 mg/1
0. 010 mg/1
0. 010 mg/1
0. 010 mg/1
0. 010 mg/1
o. 010 mg/1
0 .010 mg/1
0.010 mg/1
0. 010 mg/1
0. 010 mg/1
0.010 mg/1
0. 010 mg/1
0. 010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0. 010 mg/1
0. 010 mg/1
0 .010 mg/1
0.025 mg/1
0.010 mg/1
0 .010 mg/1
0 .010 mg/1
0. 040 mg/1
0.10 rng/1
0.0010 rng/1
0.0010 mg/1
0.0010 rng/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0 .0010 mg/1
0 . 0050 mg/1
0.0050 mg/1
0.0050 rng/1
0.0050 mg/1
April 18, 2005
Report ID: AC1040
L05022303-02
02/22/2005 1453
02/22/2005
Analyst
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
Date
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
03/03/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
Time
1515
1515
1515
1515
1515
1515
1515
1515
1515
1515
1515
1515
1515
1515
1515
1515
1515
1515
1515
1515
1515
1515
1515
1515
1515
1438
1756
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
Davis & Floyd, Inc. ! PO Drawer 428 I Greenwood, SC 29648 I fl 1 fi F.. Durst Avenue I Greenwood,. SC 29649 I (864) 2'..!~l-4413 I Fax (864) 229-71 19
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D~IS
FLOYD LABORATORY ANALYSIS REPORT
Client TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Contact Pem Carter
Client ID: PBW-3
Matrix : GW/ChemW
Parameter
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLORQBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Prep Procedure
Analytical Prep Procedures:
DOWTHERM
8270 SVOC PREP
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
Method
SW846 3500B
SW846 3510C
Result Qual
0.0010
0.0010
0.0010
0 0010
0 .0010
0 0010
0 . 0010
0.0010
0.0010
0.0010
0.0010
0 0010
0 0010
0 .0010
0. 0010
0. 0010
0. 0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0020
Analyst
DBC
DBC
NC Certification Number: 25
Project Number:
Report Date
Page 29 of 88
Sample ID
Date Collected:
Date Received
RDL Units
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0 .0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0. 002 0 mg/1
Prep Date
02/28/2005 0800
02/28/2005 0800
61621.01
April 18, 2005
Report ID: AC1040
LOS022303-02
02/22/2005 1453
02/22/2005
Analyst Date
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
PAP 02/24/2005
Time
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2964H I 816 E. Durst Avenue I Grcemvoorl, SC 2%49 I (864) 229-44.13 I Fax (864) 229-7119
I
D\VIS I
FLOYD LABORATORY ANALYSIS REPORT
I
NC Cenijicarion Number: 25
Client TICONA,LLC Project Number: I
61621. 01
2525 BLACKSBURG ROAD
I HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Contact Pem Carter Page 30 of 88 Report ID: AC1040
Client IO: PEW-4 Sample ID L05022303-03 I Date Collected: 02/22/2005 1443
Matrix : GW/ChemW Date Received 02/22/2005
Parameter Result Qual RDL Units Analyst Date Time I
semi volatile eJ:rganics
SW846 8270C I 1,2,4-TRICHLOROBENZENE < 0 .010 0.010 mg/1 JRN 03/03/2005 1557
1,2-DICHLOROBENZENE < 0. 010 0.010 mg/1 JRN 03/03/200S 1557
1,3-DICHLOROBENZENE < 0.010 0.010 mg/1 JRN 03/03/2005 1557 I 1,4-DICHLOROBENZENE < 0.010 0. 010 mg/1 JRN 03/03/2005 1557
2, 4, 5-,TRICHLOROPHENOL < 0.010 0. 010 mg/1 JRN 03/03/2005 1557
2,4,6-TRICHLOROPHENOL < 0.010 0. 010 mg/1 JRN 03/03/2005 1557
2,4-DICHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1557 I 2,4-DIMETHYLPHENOL < 0.010 0. 010 mg/1 JRN 03/03/2005 1557
2, 4-DINITROPHENOL < 0.025 0.025 mg/1 JRN 03/03/2005 1557
2,4-DINITROTOLUENE < 0.010 0.010 mg/1 JRN 03/03/2005 1557
2,6-DINITROTOLUENE < 0. 010 0 .010 mg/1 JRN 03/03/2005 1557 I 2-CHLORONAPHTHALENE < 0.010 0 .010 mg/1 JRN 03/03/2005 1557
2 -CHLOROPHENOL < 0. 010 0.010 mg/1 JRN 03/03/2005 1557
2-METHYL-4,6-DINITROPHENOL < 0 .025 0.025 mg/1 JRN 03/03/2005 1557 I 2-METHYLNAPHTHALENE < 0. 010 0 .010 mg/1 JRN 03/03/2005 1557
2-METHYLPHENOL < 0. 010 0. 010 mg/1 JRN 03/03/2005 1557
2-NITROANILINE < 0 .010 o. 010 mg/1 JRN 03/03/2005 1S57
2-NITROPHENOL < 0.010 o. 010 mg/1 JRN 03/03/2005 1557 I 3,3'-DICHLOROBENZIDINE < 0 .010 0 .010 mg/1 JRN 03/03/2005 1557
3-NITROANILINE < 0 .010 0.010 mg/1 JRN 03/03/2005 1557
4-BROMOPHENYL PHENYL ETHER < 0. 010 0.010 mg/1 JRN 03/03/2005 1557
4-CHLOR0-3-METHYLPHENOL < 0. 010 0.010 mg/1 JRN 03/03/2005 1557 I 4-CHLOROANILINE < 0.010 0.010 mg/1 JRN 03/03/2005 1557
4-CHLOROPHENYL PHENYL ETHER < 0.010 0. 010 mg/1 JRN 03/03/2005 1557
4-METHYLPHENOL < 0.010 0. 010 mg/1 JRN 03/03/2005 1557 I 4-NITROANILINE < o. 010 0.010 mg/1 JRN 03/03/2005 1557
4-NITROPHENOL < 0.025 0. 025 mg/1 JRN 03/03/2005 1557
ACENAPHTHENE < 0. 010 o. 010 mg/1 JRN 03/03/2005 1557
ACENAPHTHYLENE < o. 010 0.010 mg/1 JRN 03/03/2005 1557 I ANTHRACENE < 0 .010 0. 010 mg/1 JRN 03/03/2005 1557
BENZO(A)ANTHRACENE < 0. 010 0.010 mg/1 JRN 03/03/2005 1557
BENZO(A)PYRENE < 0 .010 0.010 mg/1 JRN 03/03/2005 1557
BENZO(B)FLUORANTHENE < 0 .010 0. 010 mg/1 JRN 03/03/2005 1557 I BENZO(G,H,I)PERYLENE < 0.010 0. 010 mg/1 JRN 03/03/2005 1557
BENZO(K)FLUORANTHENE < o. 010 0.010 mg/1 JRN 03/03/2005 1557
BENZOIC ACID < 0. 050 0 .050 mg/1 JRN 03/03/2005 1557 I BENZYL ALCOHOL < 0 .010 0. 010 mg/1 JRN 03/03/2005 1557
BIS(2-CHLOROETHOXY)METHANE < 0 .010 0. 010 mg/1 JRN 03/03/2005 1557
BIS(2-CHLOROETHYL)ETHER < 0. 010 0.010 mg/1 JRN 03/03/2005 1557
BIS(2-CHLOROISOPROPYL)ETHER < 0. 010 0.010 mg/1 JRN 03/03/2005 1557 I D,wis & Floyd, Inc. I ro Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 2%49 I (8(,4) :229-4-1 I J I Fax (864) 22lJ-7 ! 19
I
I 011s LABORATORY ANALYSIS REPORT FL 'YD I
NC Certification Number: 25
I Client TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
I HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Contact Pem Carter Page 31 of 88 Report ID: AC1040
I Client ID: PBW-4 Sample ID L05022303-03
Date Collected, 02/22/2005 1443
Matrix GW/ChemW Date Received 02/22/2005
I Parameter Result Qual RDL units Analyst Date Time
BIS{2-ETHYLHEXYL)PHTHALATE ' 0.010 0. 010 mg/i JRN 03/03/2005 1557 I BUTYL BENZYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557
CHRYSENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557
DI-N-BUTYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557
I D1-N-OCTYL PHTHALATE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1557
DIBENZ(~,H)ANTHRACENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557
DIBENZOFURAN ' 0.010 0.010 mg/1 JRN 03/03/2005 1557,
DIETHYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557
I DIMETHYL PHTHALATE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1557
FLUORANTHENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1557
FLUORENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1557
HEXACHLOROBENZENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1557
I HEXACHLOROBlITADIENE ' 0.010 o. 010 mg/1 JRN 03/03/2005 1557
HEXACHLOROCYCLOPENTADIENE ' 0.010 0 010 mg/1 JRN 03/03/2005 1557
HEXACHLOROETHANE ' 0.010 o. 010 mg/1 JRN 03/03/2005 1557
I INDENO(l,2,3-CD)PYRENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1557
ISOPHORONE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557
N-NITROSODI-N-PROPYLAMINE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557
N-NITROSODIPHENYLAMINE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557
I NAPHTHALENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557
NITROBENZENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1557
PENTACHLOROPHENOL ' 0.025 0.025 mg/1 JRN 03/03/2005 1557
PHENANTHRENE ' 0.010 0 .010 mg/1 JRN 03/03/2005 1557 I PHENOL ' 0.010 0. 010 mg/1 JRN 03/03/2005 1557
PYRENE ' 0.010 o. 010 mg/1 JRN 03/03/2005 1557
SWB46 8270C DOWTHERM
I 1,1'-BIPHENYL ' 0.010 0 .010 mg/1 JRN 03/03/2005 1557
BIPHENYL ETHER 0. 026 0.010 mg/1 JRN 03/03/2005 1557
Volatile Organics
I SW846 8260B
1,1,1-TRICHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0933
1,1,2,2-TETRACHLOROETHANE ' 0 0010 0.0010 mg/1 PAP 02/24/2005 0933
1,1,2-TRICHLOROETHANE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0933
I 1,1-DICHLOROETHANE ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 0933
1,1-DICHLOROETHBNE ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 0933
1,2-DICHLOROETHANE ' 0 0010 0.0010 mg/1 PAP 02/24/2005 0933
1,2-DICHLOROPROPANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 0933 I 2-BUTANONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0933
2-HEXANONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0933
4-METHYL-2-PENTANONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0933
I ACETONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0933
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2Yf>413 I 816 E. Durst AVt:!lllle I Greenwood, SC 2%49 I 1864) 229-4413 I Fox (864) 229-7119
Df\lIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
Client ID: PEW-4
Matrix ; GW/Chemw
Para.meter
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
OIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Prep Procedure
Analytical Prep Procedures,
DOWTHERM
8270 SVOC PREP
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
Method
SW846 35008
SW846 3510C
Result Qual
0.0026
0. 0010
0 .0010
0 .0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0056
0 .0010
0. 0010
0.0010
0. 0010
0 .0010
0 .0010
0. 0010
0.0010
0.0010
0.015
0.0010
0.0010
0.0020
Analyst
DBC
DBC
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 32 of 88
April 18, 2005
Report ID: AC1040
Sample ID L05022303-03
Date Collected: 02/22/2005 1443
Date Received 02/22/2005
RDL Units
0 .0010 mg/1
0. 0010 mg/1
0.0010 mg/1
0.0010 mg/1
0 .0010 mg/1
0 .0010 mg/1
0 .0010 mg/1
o. 0010 mg/1
0.0010 mg/1
0 .0010 mg/1
0. 0010 mg/1
0 .0010 mg/1
0. 0010 mg/1
0.0010 mg/1
0. 0010 mg/1
0 .0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0 .0010 mg/1
0. 0010 mg/1
0 .0010 mg/1
0.0010 mg/1
0.0020 mg/1
Prep Date
02/28/2005 0800
02/28/2005 0800
Analyst
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
Date
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
02/24/2005
Time
0933
0933
0933
0933
0933
0933
0933
0933
0933
093 3
0933
0933
0933
0933
0933
0933
0933
0933
0933
0933
0933
0933
0933
0933
Davis & Floyd, Inc. I PO Drawer 42B I Greenwood, SC 2%48 I 81 fi E. Durst 1\venut! I Greenwo(ld, SC 2%49 I (864) 229~44 lJ I Fax (864) 229-71 I 9
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I
DAVIS FL6YD LABORATORY ANALYSIS REPORT
NC Certification Number: 25
Client TICONA,LLC Project Number: 61621. 01
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Contact Fem Carter Page 33 of 88 Report ID: AC1040
Client ID: DUP-4 Sample ID LOS022303-04
Date Collected: 02/22/2005 0000
Matrix GW/ChemW Date Received 02/22/2005
Parameter Result Oual RDL Units Analyst Date Time
Semi volatile organics
SW846 8270C
1,2,4-TRICHLOROBENZENE < 0 .010 0.010 mg/1 JRN 03/03/2005 1636
1,2-DICHLOROBENZENE < 0 .010 0. 010 mg/1 JRN 03/03/2005 1636
1,3-DICHLOROBENZENE < 0 .010 0. 010 mg/1 JRN 03/03/2005 1636
1,4-DIC~LOROBENZENE < 0 .010 0.010 mg/1 JRN 03/03/2005 1636
2, 4, S-:tRICHLOROPHENOL < 0. 010 0. 010 mg/1 JRN 03/03/2005 1636
2,4,6-TRICHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1636
2,4-DICHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1636
2,4-DIMETHYLPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1636
2,4-DINITROPHENOL < 0. 025 0.025 mg/1 JRN 03/03/2005 1636
2,4-DINITROTOLUENE < 0.010 0.010 mg/1 JRN 03/03/2005 1636
2,6-DINITROTOLUENE < 0.010 0.010 mg/1 JRN 03/03/2005 1636
2-CHLORONAPHTHALENE < 0.010 0.010 mg/1 JRN 03/03/2005 1636
2-CHLOROPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1636
2-METHYL-4,6-DINITROPHENOL < 0.025 0. 025 mg/1 JRN 03/03/2005 1636
2-METHYLNAPHTHALENE < 0.010 0. 010 mg/1 JRN 03/03/2005 1636
2-METHYLPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1636
2-NITROANILINE < 0.010 0.010 mg/1 JRN 03/03/2005 1636
2-NITROPHENOL < 0.010 0.010 mg/1 JRN 03/03/2005 1636
3,3'-DICHLOROBENZIDINE < 0 010 0.010 mg/1 JRN 03/03/2005 1636
3-NITROANILINE < o. 010 0.010 mg/1 JRN 03/03/2005 1636
4-BROMOPHENYL PHENYL ETHER < 0 .010 0.010 mg/1 JRN 03/03/2005 1636
4 -CHLORO-3-METHYL.PHENOL < 0. 010 0.010 mg/1 JRN 03/03/2005 1636
4-CHLOROANILINE < 0. 010 0.010 mg/1 JRN 03/03/2005 1636
4-CHLOROPHENYL PHENYL ETHER < 0. 010 0.010 mg/1 JRN 03/03/2005 1636
4-METHYLPHENOL < 0.010 0 010 mg/1 JRN 03/03/2005 1636
4-NITROANILINE < 0 010 0. 010 mg/1 JRN 03/03/2005 1636
4-NITROPHENOL < 0 025 0 .025 mg/1 JRN 03/03/2005 1636
ACENAPHTHENE < 0 .010 0 .010 mg/1 JRN 03/03/2005 1636
ACENAPHTHYLENE < 0 .010 0. 010 mg/1 JRN 03/03/2005 1636
ANTHRACENE < 0.010 0.010 mg/1 JRN 03/03/2005 1636
BENZO(A)ANTHRACENE < 0.010 0.010 mg/1 JRN 03/03/2005 1636
BENZO(A)PYRENE < 0.010 0.010 mg/1 JRN 03/03/2005 1636
BENZO(B)FLUORANTHENE < 0.010 0.010 mg/1 JRN 03/03/2005 1636
BENZO{G,H,I)PERYLENE < 0. 010 0.010 mg/1 JRN 03/03/2005 1636
BENZO{K)FLUORANTHENE < 0.010 0.010 mg/1 JRN 03/03/2005 1636
BENZOIC ACID < 0.050 0.050 mg/1 JRN 03/03/2005 1636
BENZYL ALCOHOL < 0.010 0.010 mg/1 JRN 03/03/2005 1636
BIS(2-CHLOR6ETHOXY)METHANE < 0.010 0.010 mg/1 JRN 03/03/2005 1636
815(2-CHLOROETHYL)ETHER < 0.010 0 010 mg/1 JRN 03/03/2005 1636
815(2-CHLOROISOPROPYL)ETHER < 0.010 0.010 mg/1 JRN 03/03/2005 1636
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I fl 16 E. Durst Avenue I Greemvoml. SC 29649 I (864) 229-4413 I Fax (864) 229-7119
I
DAIIS I
FLOYD LABORATORY ANALYSIS REPORT
I
NC Cenijication Number: 25
I Client TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
I HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Contact Pem Carter Page 34 of 88 Report ID: AC1040
Client ID: DUP-4 Sample ID L05022303-04 I Date Collected: 02/22/2005 0000
Matrix GW/Chemw Date Received 02/22/2005
Parameter Result Qual RDL units Analyst Date Time I
BIS(2-ETHYLHEXYL)PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636 I BUTYL BENZYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636
CHRYSENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636
D1-N-BUTYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636
D1-N-OCTYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636 I DIBENZ(A_, HJ ANTHRACENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1636
DIBENZOFURAN ' 0.010 0.010 mg/1 JRN 03/03/2005 1636
DIETHYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636
DIMETHYL PHTHALATE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636 I FLUORANTHENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636
FLUORENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636
HEXACHLOROBENZENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636 I HEXACHLOROBUTADIENE ' 0. 010 o. 010 mg/1 JRN 03/03/2005 1636
HEXACHLOROCYCLOPENTADIENE ' 0.010 0 010 mg/1 JRN 03/03/2005 1636
HEXACHLOROETHANE ' 0. 010 0 010 mg/1 JRN 03/03/2005 1636
INDENO(l,2,3-CD)PYRENE ' 0.010 0 .010 mg/1 JRN 03/03/2005 1636 I ISOPHORONE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636
N-NITROSOOI-N-PROPYLAMINE ' 0.010 0.010 mg/1 JRN 03/03/2005 1636
N-NITROSOOIPHENYLAMINE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1636
NAPHTHALENE ' 0.010 0 010 mg/1 JRN 03/03/2005 1636 I NITROBENZENE ' 0.010 0 010 mg/1 JRN 03/03/2005 1636
PENTACHLOROPHENOL ' 0.025 0 .025 mg/1 JRN 03/03/2005 1636
PHENANTHRENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1636 I' PHENOL ' 0.010 0. 010 mg/1 JRN 03/03/2005 1636
PYRENE ' 0.010 0 010 mg/1 JRN 03/03/2005 1636
SW846 8270C DOWTHERM
1, l' -Bl PHENYL ' 0 .010 0 .010 mg/1 JRN 03/03/2005 1636 I BIPHENYL ETHER < 0 .010 0.010 mg/1 JRN 03/03/2005 1636
Volatile Organics
SW846 8260B I 1,1,1-TRICHLOROETHANE ' 0.0010 0 .0010 mg/1 PAP 02/24/2005 0951
1,1,2,2-TETRACHLOROETHANE ' 0 .0010 0. 0010 mg/1 PAP 02/24/2005 0951
1,1,2-TRICHLOROETHANE ' 0 .0010 0 .0010 mg/1 PAP 02/24/2005 0951
1,1-DICHLOROETHANE ' 0 .0010 0. 0010 mg/1 PAP 02/24/2005 0951 I 1,1-DICHLOROETHENE < 0 0010 0.0010 mg/1 PAP 02/24/2005 0951
1,2-DICHLOROETHANE ' 0.0010 0 0010 mg/1 PAP 02/24/2005 0951
1,2-DICHLOROPROPANE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0951 I 2-BUTANONE ' 0 .0050 0 . 0050 mg/1 PAP 02/24/2005 0951
2-HEXANONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0951
4-METHYL-2-PENTANONE ' 0 0050 0.0050 mg/1 PAP 02/24/2005 0951
ACETONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 0951 I Davis & Floyd, Inc. I PO Drawer 428 I Crecnwoorl, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (H64) 229-4.t 13 I Fax (864) 229-7119
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DAYIS
FLCWD
Client
Contact
Client
Matrix
Parllll!eter
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROB.ENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
ID:
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-0ICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Prep Procedure
Analytical Prep Procedures1
DOWTHERM
8270 SVOC PREP
LABORATORY ANALYSIS REPORT
NC Certification Number: 25
TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Pem Carter Page 35 of 88 Report ID: AC1040
DUP-4 Sample ID L05022303-04
Date Collected: 02/22/2005 0000
GW/ChemW Date Received 02/22/2005
Result Qual RDL Units Analyst Date Time
' 0. 0010 0 . 0010 mg/1 PAP 02/24/2005 0951
' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0951
' 0. 0010 0.0010 mg/1 PAP 02/24/2005 0951
' 0 .0010 0.0010 mg/1 PAP 02/24/2005 0951
' 0. 0010 0 . 0010 mg/1 PAP 02/24/2005 0951
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951
0.0018 0.0010 mg/1 PAP 02/24/2005 0951
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951
0.0012 0.0010 mg/1 PAP 02/24/2005 0951
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951
0.0054 0.0010 mg/1 PAP 02/24/2005 0951
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951
' 0.0010 0.0010 mg/1 PAP 02/24/2005 0951
' 0.0020 0.0020 mg/1 PAP 02/24/2005 0951
Method Analyst Prep Date
SW846 35008 DBC 02/28/2005 0800
SW846 3510C DBC 02/28/2005 0800
Davis 8, Floyd. Inc. I PO Drawer 42a I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood. SC 2%49 I (864) 229-441 :I I Fax (864) 229-7119
DA.YIS FL6YD LABORATORY ANALYSIS REPORT
NC Certification Number: 25
Client TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Contact Pem Carter Page 36 of 88 Report ID: AC1040
Client ID: TRIP BLANK-3 Sample ID L05022303-05
Date Collected: 02/08/2005 0900
Matrix : GW/ChemW Date Received 02/22/2005
Parameter Result Qual RDL Units Analyst Date Time
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE < 0 .0010 0 .0010 mg/1 PAP 02/24/2005 0801
1,1,2,2-TETRACHLOROETHANE < o. 0010 0 .0010 mg/1 PAP 02/24/2005 0801
1,1,2-TRICHLOROETHANE < 0 .0010 o. 0010 mg/1 PAP 02/24/2005 0801
1,1-Dl~LOROETHANE < 0 .0010 o. 0010 mg/1 PAP 02/24/2005 0801
1,1-DICHLOROETHENE < o. 0010 0. 0010 mg/1 PAP 02/24/2005 0801
1,2-DICHLOROETHANE < 0. 0010 0. 0010 mg/1 PAP 02/24/2005 0801
l,2-DICHLOROPROPANE < 0. 0010 0 . 0010 mg/1 PAP 02/24/2005 0801
2-BUTANONE < 0 .0050 0.0050 mg/1 PAP 02/24/2005 0801
2-HEXANONE < 0 .0050 0.0050 mg/1 PAP 02/24/2005 0801
4-METHYL-2-PENTANONE < 0 .0050 0.0050 mg/1 PAP 02/24/2005 0901
ACETONE < 0.0050 0.0050 mg/1 PAP 02/24/2005 0801
BENZENE < 0. 0010 o. 0010 mg/1 PAP 02/24/2005 0801
BROMODICHLOROMETHANE < 0 .0010 0 .0010 mg/1 PAP 02/24/2005 0801
BROMOFORM < o. 0010 0 .0010 mg/1 PAP 02/24/2005 0801
BR OMO METHANE < 0 .0010 o. 0010 mg/1 PAP 02/24/2005 0801
CARBON DISULFIDE < 0.0010 0.0010 mg/1 PAP 02/24/2005 0801
CARBON TETRACHLORIDE < 0. 0010 0 .0010 mg/1 PAP 02/24/2005 0801
CHLOROBENZENE < 0 .0010 0 .0010 mg/1 PAP 02/24/2005 0801
CHLOROETHANE < 0 .0010 0 .0010 mg/1 PAP 02/24/2005 0801
CHLOROFORM < 0.0010 0.0010 mg/1 PAP 02/24/2005 0801
CHLOROMETHANE < 0.0010 0.0010 mg/1 PAP 02/24/2005 0801
CIS-1,2-DICHLOROETHENE < 0 .0010 0.0010 mg/1 PAP 02/24/2005 0801
CIS-1,3-DICHLOROPROPENE < 0. 0010 0.0010 mg/1 PAP 02/24/2005 0801
DIBROMOCHLOROMETHANE < 0. 0010 0.0010 mg/1 PAP 02/24/2005 0801
ETHYLBENZENE < 0 .0010 0.0010 mg/1 PAP 02/24/2005 0901
METHYLENE CHLORIDE < 0 .0010 0.0010 mg/1 PAP 02/24/2005 0801
STYRENE < 0 .0010 0.0010 mg/1 PAP 02/24/2005 0801
TETRACHLOROETHENE < 0' 0010 0.0010 mg/1 PAP 02/24/2005 0801
TOLUENE < 0 .0010 0.0010 mg/1 PAP 02/24/2005 0801
TRANS-1,2-DIOILOROETHENE < 0 .0010 0.0010 mg/1 PAP 02/24/2005 0801
TRANS-1,J-DICHLOROPROPENE < 0 .0010 0.0010 mg/1 PAP 02/24/2005 0801
TRICHLOROETHENE < 0.0010 0.0010 mg/1 PAP 02/24/2005 0801
VINYL ACETATE < 0.0010 0.0010 mg/1 PAP 02/24/2005 0801
VINYL CHLORIDE < 0.0010 0.0010 mg/1 PAP 02/24/2005 0801
XYLENE (TOTAL) < 0.0020 0.0020 mg/1 PAP 02/24/2005 0801
0;ivis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2%48 I 8 I 6 E. Durst Avenue I Greenwood, SC 2%49 I (864) 229-4413 j F.ix (H(i4) 229-7119
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DAVIS
FL6'YD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
Client IO: V-23
Matrix : GW/Chemw
Para.meter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-D~CHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Wet Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
Result Qual
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0050
0.0050
0.0050
0.0050
0. 021
0.0010
0.0010
0.0010
0 0010
0 0010
0.0010
0.0010
0.0010
0.0010
0 0010
0 0010
0.0010
0. 0031
0.0010
0.0010
0.0010
0.010
0.0010
0.0010
0.0010
0.0010
0.0010
0.012
10700
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 37 of as
April 18, 2005
Report ID: AC1040
Sample ID L05022401-0l
Date Collected: 02/23/2005 0945
Date Received 02/23/2005
RDL
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0050
0.0050
0.0050
0.0050
0.0010
0.0010
0.0010
0.0010
0.0010
0 0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0. 0010
0.0010
0.0020
500
Units
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Analyst
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
CDC
Date Time
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 124.6
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
02/24/2005 1246
03/03/2005 2002
Davis & Floyd, Inc. I PO Draw~r 428 ] Greenwood, SC 2%4fl I 81 G f:. Dui·st Avenw: I Greenwood. SC 29h49 I W64) 229-4413 I Fax (8G4) 229-71 19
D~IS
FLMD
Client
Contact
Client ID:
Matrix
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-0ICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Wet Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
LABORATORY ANALYSIS REPORT
NC Certification Number: 25
TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Pem Carter Page 38 of 88 Report ID: AC1040
K-28 Sample ID L05022401-02
Date Collected, 02/22/2005 1715
GW/Chemw Date Received 02/23/2005
Result Qual RDL Units Analyst Date Time
' 0.0010 0.0010 mg/1 PAP 02/24/2005 1343
' 0.0010 0.0010 mg/1 PAP 02/24/2005 1343
' 0.0010 0.0010 mg/1 PAP 02/24/2005 1343
' 0.0010 0.0010 mg/1 PAP 02/24/2005 1343
' 0.0010 0.0010 mg/1 PAP 02/24/2005 1343
' 0. 0010 0.0010 mg/1 PAP 02/24/2005 1343
' 0. 0010 0.0010 mg/1 PAP 02/24/2005 1343
0.084 0.0050 mg/1 PAP 02/24/2005 1343
' 0. 0050 0.0050 mg/1 PAP 02/24/2005 134 3
' 0.0050 0 . 0050 mg/1 PAP 02/24/2005 1343
0.12 0 . 0050 mg/1 PAP 02/24/2005 1343
0.0083 0. 0010 mg/1 PAP 02/24/2005 1343
' 0.0010 0 .0010 mg/1 PAP 02/24/2005 1343
' 0.0010 0.0010 mg/1 PAP 02/24/2005 1343
' 0 .0010 0. 0010 mg/1 PAP 02/24/2005 1343
' 0 .0010 0. 0010 mg/1 PAP 02/24/2005 1343
' 0 .0010 o. 0010 mg/1 PAP 02/24/2005 1343
' o. 0010 0.0010 mg/1 PAP 02/24/2005 1343
' o. 0010 0.0010 mg/1 PAP 02/24/2005 1343
' 0.0010 0.0010 mg/1 PAP 02/24/2005 1343
' 0 .0010 0.0010 mg/1 PAP 02/24/2005 1343
' o. 0010 0. 0010 mg/1 PAP 02/24/2005 1343
' 0 .0010 0. 0010 mg/1 PAP 02/24/2005 1343
' 0.0010 0 .0010 mg/1 PAP 02/24/2005 1343
' 0.0010 0. 0010 mg/1 PAP 02/24/2005 1343
' 0.0010 0. 0010 mg/1 PAP 02/24/2005 1343
' 0.0010 0.0010 mg/1 PAP 02/24/2005 1343
' o._0010 0.0010 mg/1 PAP 02/24/2005 1343
0.0020 0.0010 mg/1 PAP 02/24/2005 1343
' 0.0010 0.0010 mg/1 PAP 02/24/2005 1343
' 0.0010 0 . 0010 mg/1 PAP 02/24/2005 1343
' 0.0010 0 . 0010 mg/1 PAP 02/24/2005 1343
' 0.0010 0 .0010 mg/1 PAP 02/24/2005 1343
' 0. 0010 0 . 0010 mg/1 PAP 02/24/2005 1343
' 0. 0020 0 . 0020 mg/1 PAP 02/24/2005 1343
60.4 12.s mg/1 CDC 03/03/2005 2027
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2J648 I 816 E. Durst Avenue I Grecnwnod, SC 29649 I (804) 229-441 :i I Fax (864) 229-7 J 19
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LABORATORY ANALYSIS REPORT
I
I
NC Cenijication Number: 25
Client TICONA,LLC Project Number: 61621.01
I 2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Contact Pem Carter Page 39 of 88 Report ID: AC1040
I Client ID: TRIP BLANK-4 Sample ID L05022401-03
Date Collected: 02/08/2005 0900
Matrix GW/ChemW Date Received 02/23/2005
I Parameter Result Qual RDL units Analyst Date Time
I Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227
1,1,2,2-TETRACHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227
I 1,1,2-TRICHLOROETHANE ' 0.0010 0. 0010 mg/1 PAP 02/24/2005 1227
1,1-DIC~LOROETHANE ' 0.0010 o. 0010 mg/1 PAP 02/24/2005 1227
1,1-DICHLOROETHENE ' 0 0010 0 .0010 mg/1 PAP 02/24/2005 1227
1,2-DICHLOROETHANE ' 0 0010 0. 0010 mg/1 PAP 02/24/2005 1227
I 1,2-DICHLOROPROPANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227
2-BUTANONE ' 0 0050 0.0050 mg/1 PAP 02/24/2005 1227
2-HEXANONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 1227
I
4-METHYL-2-PENTANONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 1227
ACETONE ' 0.0050 0.0050 mg/1 PAP 02/24/2005 1227
BENZENE ' o. 0010 0.0010 mg/! PAP 02/24/2005 1227
BROMODICHLOROMETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227
I BROMOFORM ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227
BROMOMETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227
CARBON DISULFIDE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227
CARBON TETRACHLORIDE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227
I CHLOROBENZENE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227
CHLOROETHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227
CHLOROFORM ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227
I
CHLO RO METHANE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227
CIS-1,2-DICHLOROETHENE ' 0.0010 0.0010 mg/1 PAP 02/24/2005 1227
CIS-1,3-DICHLOROPROPENE ' 0.0010 0. 0010 mg/1 PAP 02/24/2005 1227
DIBROMOCHLOROMETHANE ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 1227
I ETHYLBENZENE ' 0 0010 0.0010 mg/1 PAP 02/24/2005 1227
METHYLENE CHLORIDE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 1227
STYRENE ' 0. 0010 0.0010 mg/1 PAP 02/24/2005 1227
TETRACHLOROETHENE ' 0,0010 0. 0010 mg/1 PAP 02/24/2005 1227
I TOLUENE ' 0 .0010 0.0010 mg/1 PAP 02/24/2005 1227
TRANS-1,2-DICHLOROETHENE ' 0 0010 0.0010 mg/1 PAP 02/24/2005 1227
TRANS-1,3-DICHLOROPROPENE ' o. 0010 0.0010 mg/1 PAP 02/24/2005 1227
I
TRICHLOROETHENE ' 0. 0010 0.0010 mg/! PAP 02/24/2005 1227
VINYL ACETATE ' 0 0010 0.0010 mg/1 PAP 02/24/2005 1227
VINYL CHLORIDE ' 0.0010 0 . 0010 mg/1 PAP 02/24/2005 1227
XYLENE (TOTAL} ' 0.0020 0.0020 mg/1 PAP 02/24/2005 1227
I
I Dc1vis 81 Floyd, Inc. I PO DrJwer 428 I Greenwood, SC 29()4/j I 816 E. Durst Avenue I Greenwood, SC 29649 I (8(i4l 22:.J-441 J I Fax (864) 229-7119
(' I ' ,,
DAYIS I
FL6YD LABORATORY ANALYSIS REPORT
I
NC Cenification Number: 25
I Client TICONA,LLC Project Number: 61621.01
2525 BLACKSBURG ROAD I HWY 198
SHELBY, NC 28152 Report Date April 18, 2005
Contact Pem Carter Page 40 of 88 Report ID: AC1040
Client ID: PB-01 Sample ID L05022812-0l I Date Collected: 02/22/2005 1745
Matrix : GW/ChemW Date Received 02/24/2005
Parameter Result Qual RDL Units Analyst Date Time I
Somivolatile Organics
I SW846 8270C
1,2,4-TRICHLOROBENZENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1715
1,2-DICHLOROBENZENE ' 0 .010 0 .010 mg/1 JRN 03/03/2005 1715
1,3-DICHLOROBENZENE ' 0 .010 0 .010 mg/1 JRN 03/03/2005 1715 I 1, 4-DICH_LOROBENZENE ' 0 .010 0.010 mg/1 JRN 03/03/2005 1715
2, 4, 5-.TRICHLOROPHENOL ' 0' 010 0. 010 mg/1 JRN 03/03/2005 1715
2,4,6-TRICHLOROPHENOL ' 0 .010 0.010 mg/1 JRN 03/03/2005 1715
2,4-0ICHLOROPHENOL ' 0.010 0. 010 mg/1 JRN 03/03/2005 1715 I 2,4-0IMETHYLPHENOL ' 0.010 0.010 mg/1 JRN 03/03/2005 1715
2,4-DINITROPHENOL ' 0. 025. 0.025 mg/1 JRN 03/03/2005 1715
2,4-DINITROTOLUENE ' 0.010 0.010 mg/1 JRN 03/03/2005 1715
2,6-DINITROTOLUENE ' 0.010 0, 010 mg/1 JRN 03/03/2005 1715 I 2-CHLORONAPHTHALENE ' 0 .010 0 .010 mg/1 JRN 03/03/2005 1715
2-CHLOROPHENOL ' 0, 010 0 .010 mg/1 JRN 03/03/2005 1715
2-METHYL-4,6-DINITROPHENOL ' o, 025 0 .025 mg/1 JRN 03/03/2005 1715 I 2-METHYLNAPHTHALENE ' 0' 010 0, 010 mg/1 JRN 03/03/2005 1715
2-METHYLPHENOL ' 0.010 0, 010 mg/1 JRN 03/03/2005 1715
2-NITROANILINE ' 0. 010 0. 010 mg/1 JRN 03/03/2005 1715
2-NITROPHENOL ' 0. 010 0. 010 mg/1 JRN 03/03/2005 1715 I 3,3'-DICHLOROBENZIDINE ' 0. 010 0.010 mg/1 JRN 03/03/2005 1715
3-NITROANILINE ' 0 .010 0. 010 mg/1 JRN 03/03/2005 1715
4-BROMOPHENYL PHENYL ETHER ' 0 .010 0.010 mg/1 JRN 03/03/2005 1715
4-CHLOR0-3-METHYLPHENOL ' 0 .010 0. 010 mg/1 JRN 03/03/2005 1715 I 4-0ILOROANILINE ' o, 010 0.010 mg/1 JRN 03/03/2005 1715
4 -CHLOROPHENYL PHENYL ETHER ' 0.010 0' 010 mg/1 JRN 03/03/2005 1715
4-METHYLPHENOL ' 0. 010 o, 010 mg/1 JRN 03/03/2005 1715 I 4-NITROANILINE ' 0 .010 0 .010 mg/1 JRN 03/03/2005 1715
4-NITROPHENOL ' 0 . 025 0' 025 mg/1 JRN 03/03/2005 1715
ACENAPHTHENE ' 0' 010 0.010 mg/1 JRN 03/03/2005 1715
ACENAPHTHYLENE ' 0 .010 0. 010 mg/1 JRN 03/03/2005 1715 I ANTHRACENE ' 0 .010 0.010 mg/1 JRN 03/03/2005 1715
BENZO(A)ANTHRACENE ' 0.010 0. 010 mg/1 JRN 03/03/2005 1715
BENZO (Al PYRENE ' 0, 010 0.010 mg/1 JRN 03/03/2005 1715
BENZO{B)FLUORANTHENE ' 0' 010 0.010 mg/1 JRN 03/03/2005 1715 I BENZO{G,H,I)PERYLENE ' 0' 010 0.010 mg/1 JRN 03/03/2005 1715
BENZO{K)FLUORANTHENE ' 0 .010 0. 010 mg/1 JRN 03/03/2005 1715
BENZOIC ACID ' 0 .050 0.050 mg/1 JRN 03/03/2005 1715 I BENZYL ALCOHOL ' 0, 010 0.010 mg/1 JRN 03/03/2005 1715
BIS{2-CHLOROETHOXY)METHANE ' 0' 010 0.010 mg/1 JRN 03/03/2005 1715
BIS{2-CHLOROETHYL)ETHER ' 0' 010 0.010 mg/1 JRN 03/03/2005 1715
BIS(2-CHLOROISOPROPYL)ETHER ' 0 .010 0. 010 mg/1 JRN 03/03/2005 1715 I Davis & Floyd, Inc. I PO Drawer 42H I Gr·ccnw()od, SC 2%48 I 816 E, Durst Avenue I Grecnwond, SC 2%49 I (864) 2'.!.'.)-4413 I Fax (/\(A) 229-71 1 ~l
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DAVIS FL6YD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
Client ID: FB-01
Matrix
Parameter
BIS(2-ETHYLHEXYL)PHTHALATE
BUTYL BENZYL PHTHALATE
CHRYSENE
DI-N-BUTYL PHTHALATE
DI-N-OCTYL PHTHALATE
DIBENZ (A., H) ANTHRACENE
DIBENZOFURAN
DIETHYL PHTHALATE
DIMETHYL PHTHALA.TE
FLUORANTHENE
FLUORENE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROCYCLOPENTADIENE
HEXACHLOROETHANE
INDENO(l,2,3-CD)PYRENE
ISOPHORONE
N-NITROSODI-N-PROPYLAMINE
N-NITROSODIPHENYLAMINE
NAPHTHALENE
NI TROBENZENE
PENTACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRENE
SW846 8270C DOWTHERM
1,1'-BIPHENYL
BIPHENYL ETHER
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
l,1-0ICHLOROETHANE
l,l-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
GW/ChemW
Result Qual
0. 010
0. 010
0. 010
0.010
0.010
0.010
0.010
0. 010
0.010
0. 010
0.010
0.010
0.010
0.010
0.010
0.010
0.010
0.010
0.010
0.010
0. 010
0.025
0.010
0.010
0.010
0.010
0 010
1.0
1.0
1.0
1.0
1.0
1. 0
1.0
s.o
5.0
5.0
16.2
NC Cenijication Number: 25
Project Number: 61621.01
Report Date
Page 41 of 88
April 18, 2005
Report ID: AC1040
Sample ID L05022812-01
Date Collected: 02/22/2005 1745
Date Received
RDL
0.010
0 010
0 010
0.010
0.010
0.010
0.010
0.010
0.010
0. 010
0.010
0.010
0.010
0.010
0.010
0.010
0.010
0. 010
0.010
0.010
0. 010
0.025
0.010
0.010
0.010
0.010
0.010
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
s.o
s.o
5.0
units
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
rng/1
rng/1
mg/1
rng/1
mg/1
rng/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
02/24/2005
Analyst
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
JRN
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
Date Tima
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1715
03/03/2005 1216
03/03/2005 1216
03/03/2005 1216
03/03/2005 1216
03/03/2005 1216
03/03/2005 1216
03/03/2005 1216
03/03/2005 1216
03/03/2005 1216
03/03/2005 1216
03/03/2005 1216
Davis & Floyd, Inc. I PO Dr;n.ver· 428 j Greenwood, SC 2%48 I H ! 6 L Durst 1\venuc I Creenwond, SC 2964'.) I (HF,4) 129-44 ! :1 I Fax (8G4) 229-711 ~J
DAJIS
FLOYD
Client
Contact
Client
Matrix
Parameter
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON T/:=TRACHLORIDE
CHLOR08ENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
ID:
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TETRAHYDROFURAN
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Prep Procedure
Analytical Prep Procedures,
DOWTHERM
8270 SVOC PREP
LABORATORY ANALYSIS REPORT
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
P'B-01
GW/ChemW
<
<
<
<
<
'
<
<
<
<
<
<
<
<
<
<
<
<
<
<
'
<
<
<
<
Method
SW846 35008
SW846 3510C
Result Qual
1.0
.0
.0
1 .o
1.0
1.0
1.0
.o
1 .o
1 .o
1 .o
.0
1 .o
1 .0
1 .0
1.0
1.0
5. 0
1 .o
1 .o
1 .o
1. 0
1.0
1.0
2.0
Analyst
DBC
DBC
NC Certification Number: 25
Project Number: 61621.01
Report Date April 18, 2005
Page 42 of 88 Report ID: AC1040
Sample ID L05022812~01
Date Collected: 02/22/2005 1745
Date Received 02/24/2005
RDL Units Analyst Date Time
1 .o ug/1 PAP 03/03/2005 1216
1 .o ug/1 PAP 03/03/2005 1216
1 .o ug/1 PAP 03/03/2005 1216
1.0 ug/1 PAP 03/03/2005 1216
.0 ug/1 PAP 03/03/2005 1216
1 .o ug/1 PAP 03/03/2005 1216
1 .0 ug/1 PAP 03/03/2005 1216
1. 0 ug/1 PAP 03/03/2005 1216
1.0 ug/1 PAP 03/03/2005 1216
1.0 ug/1 PAP 03/03/2005 1216
1.0 ug/1 PAP 03/03/2005 1216
1.0 ug/1 PAP 03/03/2005 1216
1.0 ug/1 PAP 03/03/2005 1216
1.0 ug/1 PAP 03/03/2005 1216
1 .o ug/1 PAP 03/03/2005 1216
1 .0 ug/1 PAP 03/03/2005 1216
1 .0 ug/1 PAP 03/03/2005 1216
5.0 ug/1 PAP 03/03/2005 1216
1.0 ug/1 PAP 03/03/2005 1216
1.0 ug/1 PAP 03/03/2005 1216
1.0 ug/1 PAP 03/03/2005 1216
1 .0 ug/1 PAP 03/03/2005 1216
1 .0 ug/1 PAP 03/03/2005 1216
1.0 ug/1 PAP 03/03/2005 1216
2.0 ug/1 PAP 03/03/2005 1216
Prep Date
02/28/2005 0800
02/28/2005 0800
Davis &-Floyd, Inc. I PO Drawe1· 428 I Creenwoorl, SC 29(i413 I BI h E. Durst Avenue I CrC'enwornl, SC 2%4') I (864) 229-44 lJ I Fax ((H)4) 22:J-7 I 19
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DAVIS
FLijYD
Client
Contact
LABORATORY ANALYSIS REPORT
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Cenijication Number: 25
Project Number: 61621.01
Report Date April 18, 2005
Page 43 of 88 Report ID: AC1040
QC Summary Data
Davis & floyU, Inc. I PO Drawer 4'..:H I Greenwood, SC 29648 I BI fi E. Durst Avenue I Greenwood, SC '..:'."Jh4<) I (1.l(i4J :!.2':l-4413 I Fax (864) 229-711 lJ
D\VIS
FLOYD LABORATORY ANALYSIS REPORT
Sample ID
L05022007-01
L05022007-02
L05022007-03
L05022007-04
Client
Contact
TICONA, LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem carter
NC Cenijication Number: 25
Project Number: 61621.01
Report Date
Page 44 of 88
April 18, 2005
Report ID: AC1040
QC Batch Report -Batch Sample List
WorkGroup WG40376 Matrix GW/ChemW
D~scription: vo/8260/TCL Prep Method
Analtyical Method: SW846 82608
PREP ANALYTICAL
Client ID •=• Date Time Date Time Analyst
P-58 02/21/2005 1544 PAP
F-55 02/21/2005 1620 PAP
CC-33 02/21/2005 1602 PAP
TRIP BLANK-2 1 02/21/2005 1204 PAP
Dilution
3
1
D;wis & Floyd, Inc. I PO Drawe,· 4:W I GrL•e11wood, SC 1%48 I Ii 16 E. Durst Avenue I Creenwoud, SC 2%-f9 I (H64) 229-441 J I Fax (WA) 229-71 19
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DAYIS
FLfiYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 45 of 88
April 18, 2005
Report ID: AC1040
QC Batch Report -Surrogates % Recovery
WorkGroup: WG40376 Matrix GW/ChemW
Prep Method
Analtyical Method: $W846 8260B
L05022007-01 02/21/2005 1544 117 105 98
LOS022007-02 02/21/2005 1620 113 107 96
L05022007-03 02/21/2005 1602 122 105 98
L05022007-04 02/21/2005 12 04 101 103 100
DCE 1,2-DICHLOROETHANE-D4
BFB BROMOFLUOROBENZENE
TOL TOLUENE-DB
Davis 8, Floyd, Inc. I PO Drawer 42H I Creenwood, SC 2%48 I l.l I (j t. Dur~I Avenue I Greenwood, SC L:l(i4~) I (864) 229-44 fJ I Fax (1364) 229-711 '.l
D~fIS FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Cenification Number: 25
Project Number: 61621.01
Report Date April 18, 2005
Page 46 of 88 Report ID: AC1040
QC Batch Report -Batch Sample List
WorkGroup WG40399 Matrix GW/Chemw
D~scription: VO/8260/TCL RDL OF' 1 Prep Method
Analtyical Method: SW846 82608
ANALYTICAL
Sample ID Client ID Rud
PRP!P
Date Time Date Time Analyst Dilution
105021805-01 HH-77
L05021805-02 HH-48
105021805-03 C-49
105021805-04 FF-34
L05021805-05 FF-62
L05021805-06 GG-61
105021805-07 T-35
105021805-08 AA-54
L05021805-09 EE-58
MB40399:l Method Blank
LCS40399:l Laboratory Control Spike
MS05021805-03 :40399 Matrix Spike
MSD05021805-03:40399 Matrix Spike Duplicate
1 02/22/2005
1 02/22/2005
1 02/22/2005
1 02/22/2005
02/22/2005
1 02/22/2005
02/22/2005
1 02/22/2005
1 02/22/2005
02/22/2005
02/22/2005
02/22/2005
02/22/2005
1556
1328
1346
1405
1424
1442
1501
1519
1538
1033
1729
1634
1652
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
PAP
1
1
1
1
1
D,1vis &-Floyd, Inc. I PO Drnwer 4213 I Greenwood, SC 2%48 I 81 h E. Durst Aventie I Greenwood, SC 29fi49 I /864\ n9-44 1 J I F::ix (llli4) 22Y-7 I I~
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DAVIS FL61'D LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Fem Carter
NC Certification Number: 25
Project Number: 61621.01
Report Date April 18, 2005
Page 47 of BB Report ID: AC1040
QC Batch Report -Surrogates % Recovery
WorkGroup: WG40399 Matrix GW/ChemW
Prep Method
Analtyical Method: SWB46 82608
L05021805-01 02/22/2005 1556 105 99 96
L05021805-02 02/22/2005 1328 95 97 97
L05021805-03 02/22/2005 1346 96 98 97
L05021805-04 02/22/2005 1405 99 100 98
L05021805-05 02/22/2005 1424 98 99 98
L05021805-06 02/22/2005 1442 97 99 97
L05021805-07 02/22/2005 1501 101 101 98
L05021805-08 02/22/2005 1519 100 99 98
L05021805-09 02/22/2005 1538 99 99 98
MB40399:l 02/22/2005 1033 97 98 99
LCS40399:1 02/22/2005 1729 118 104 95
MS05021805-03:40399 02/22/2005 1634 114 101 96
MSD05021805-03:40399 02/22/2005 1652 115 100 96
DCE 1,2-DICHLOROETHANE-D4
BFB BROMOFLUOROBENZENE
TOL TOLUENE-DB
O;wis & Floyd, Inc. I PO Druwer 428 I Greenwood, SC 29648 I Bl 6 E. Durst /\venue I Greenwood, SC 2%-+9 I (864) 229-4413 I Fax (864) 229-7119
DAYIS Filrvo LABORATORY ANALYSIS REPORT
Client
Contact
TICONA, LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem carter
QC Batch Report-Method Blanks
WorkGroup: WG40399
B~ank MB40399:1
Para.motor Result Qual
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE < 0.0010
1 , 1, 2 , 2 -_TETRACHLOROETHANE < 0.0010
l,l,2~TRIC1-iLOROETHANE < 0. 0010
1,1-DICHLOROETHANE < 0.0010
1,1-DICHLOROETHENE < 0.0010
1,2-DICHLOROETHANE < 0.0010
1,2-DICHLOROPROPANE < 0.0010
2-BUTANONE < 0.0050
2-HEXANONE < 0.0050
4-METHYL-2-PENTANONE < 0. 0050
ACETONE < 0 0050
BENZENE < 0 0010
BROMODICHLOROMETHANE < 0. 0010
BROMOFORM < 0.0010
BROMOMETHANE < 0 0010
CARBON DISULFIDE < 0 0010
CARBON TETRACHLORIDE < 0 .0010
CHLOROBENZENE < 0 .0010
CHLOROETHANE < 0 0010
CHLOROFORM < o. 0010
CHLOROMETHANE < 0.0010
CIS-1,2-DICHLOROETHENE < 0.0010
CIS-1,3-DICHLOROPROPENE < 0.0010
DIBROMOCHLOROMETHANE < 0.0010
ETHYLBENZENE < 0.0010
METHYLENE CHLORIDE < 0 0010
STYRENE < 0.0010
TETRACHLOROETHENE < 0.0010
TOLUENE < 0.0010
TRANS-1,2-DICHLOROETHENE < 0.0010
TRANS-1,3-DICHLOROPROPENE < 0.0010
TRICHLOROETHENE < 0.0010
VINYL ACETATE < 0.0010
VINYL CHLORIDE < 0.0010
XYLENE (TOTAL) < 0.0020
NC Cenijication Number: 25
Project Number: 61621.01
Report Date
Page 48 of 88
Matrix: GW/Chemw
RDL Units
0 . 0010 mg/1
0. 0010 mg/1
0. 0010 mg/1
0 .0010 mg/1
0. 0010 mg/1
0 0010 mg/1
0.0010 mg/1
0.0050 mg/1
0.0050 mg/1
0.0050 mg/1
0.0050 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/!
0.0010 mg/1
0.0010 mg/1
0.0010 mg/!
0 0010 mg/1
0 .0010 mg/1
0. 0010 mg/1
0 0010 mg/1
0.0010 rng/1
0.0010 rng/1
0.0010 mg/1
0.0010 mg/1
0.0010 rng/1
0.0010 rng/1
0.0010 rng/1
0.0010 rng/1
0.0010 rng/1
0.0010 rng/1
0.0010 mg/!
0.0010 rng/1
0.0020 rng/1
April 18, 2005
Report ID: AC1040
Analyst Date
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02 /22 /2 005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02 /22 /2 005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
PAP 02/22/2005
Time
1033
1033
1033
1033
1033
1033
1033
1033
1033
1033
1033
1033
1033
1033
1033
1033
1033
1033
1033
1033
1033
1033
1033
1033
1033
1033
103 3
1033
1033
1033
1033
1033
1033
1033
1033
D.ivis &· Floyd, Inc. I PO Drawer 42R I Greenwood, SC 29648 I 81 h E. Durst Avenue I Greenwood, SC 29649 I (86·1) 229-4413 I Fax (864) 229-7 ! 1 Y
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DAVIS FL6YD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Cenijication Number: 25
Project Number, 61621.01
Report Date
Page 49 of as
April 18, 2005
Report ID: AC1040
QC Batch Report -Matrix Spikes and Duplicates
WorkGroup: WG40399
MS/MSD MS0S0:21805-03: 40399
MSD05021805-03:40399
1,1,1-TRICHLOROETHANE 0.0500
1,1,2-TRICHLOROETHANE 0.0500
1, 1-DICH_LOROETHENE 0.0500
1,2-DioiLOROETHANE 0.0500
1,2-DICHLOROPROPANE 0.0500
2-BUTANONE 0.0500
BENZENE 0.0500
CARBON TETRACHLORIDE 0.0500
CHLOROBENZENE 0.0500
CHLOROFORM 0.0500
DIBROMOCHLOROMETHANE 0.0500
TETRACHLOROETHENE 0.0500
TOLUENE 0.0500
TRICHLOROETHENE 0.0500
VINYL CHLORIDE 0.0500
1,1,1-TRICHLOROETHANE 0.0500
1,1,2-TRICHLOROETHANE 0.0500
1,1-DICHLOROETHENE 0.0500
1,2-DICHLOROETHANE 0.0500
1,2-DICHLOROPROPANE 0.0500
2-BUTANONE 0.0500
BENZENE 0.0500
CARBON TETRACHLORIDE 0.0500
CHLOROBENZENE 0.0500
CHLOROFORM 0.0500
DIBROMOCHLOROMETHANE 0.0500
TETRACHLOROETHENE 0.0500
TOLUENE 0.0500
TRICHLOROETHENE 0.0500
VINYL CHLORIDE 0.0500
NOTB1 MS/MSD \ recoveries are not evaluated if the
Matrix GW/Chemw
Prep Method
Analtyical Method: SWB46 8260B
< 0.00100 0.0517 mg/1 103 88-124
< 0.00100 0. 0-481 mg/1 96 88-128
< 0.00100 0.0566 mg/1 ll3 71-130
< o. 00100 0.0541 mg/1 108 78-143
< 0 .00100 0. 0455 mg/1 91 91-118
< 0. 00500 0. 0477 mg/1 95 28-199
< o. 00100 0.0514 mg/1 103 77-123
< 0. 00100 0.0557 mg/1 lll 63-135
< 0.00100 0. 04 98 mg/1 100 78-123
< 0.00100 0.0558 mg/1 ll2 75-135
< 0.00100 0.0526 mg/1 105 88-133
< 0.00100 0.0508 mg/1 102 69-123
< 0.00100 0. 04 96 mg/1 99 85-117
< 0.00100 0.0499 mg/1 100 75-121
< 0.00100 0. 0453 mg/1 91 47-136
0.0550 mg/1 llO 6 15 88-124
0. 04 94 mg/1 99 3 17 88-128
0.0584 mg/1 ll7 3 17 71-130
0.0552 mg/1 110 2 20 78-143
0.0456 mg/1 91 0 14 91-118
0.0468 mg/1 94 2 31 28-199
0.0509 mg/1 102 17 77-123
0.0576 mg/1 ll5 3 20 63-135
0.0512 mg/1 102 3 17 78-123
0.0580 mg/1 ll6 4 17 75-135
0.0543 mg/1 109 15 88-133
0.0523 mg/1 105 3 17 69-123
0.0509 mg/1 102 3 15 85-117
0.0513 mg/1 103 3 17 75-121
0. 04 64 mg/1 93 2 19 47-136
sample concentration is greater than four times the spike added.
Dcivis & Floyd, Inc. I PO Drawer 42R I Greenwood, SC 29648 I S-1 (1 F.. Durst Avenue I Creenwoud, SC 2%4~ I (864) 22~)-441 J I Fax (864) 229-7119
D~lS
FLtJYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page SO of 88
April 18, · 2005
Report ID: AC1040
QC Batch Report -Laboratory Control Standards and Duplicates
WorkGroup: WG40399 Matrix GW/ChemW
L~S LCS40399:l Prep Method
Analtyical Method: SW846 8260B
1,1,1-TRICHLOROETHANE 0.0200 0.0228 mg/1 114 79-127
1,1,2-TRICHLOROETHANE 0.0200 0 0208 mg/1 104 B3-143
1,1-DICHLOROETHENE 0 0200 0.0244 mg/1 122 63-141
1,2-DICHLOROETHANE o. 0200 0. 024 0 mg/1 120 79-147
1,2-DICHLOROPROPANE 0 . 0200 0.0187 mg/1 93 86-130
2-BUTANONE 0 0200 0 .0215 mg/1 107 52-190
BENZENE 0 .0200 0. 0217 mg/1 109 78-123
CARBON TETRACHLORIDE 0. 0200 0.0235 mg/1 117 58-132
CHLOROBENZENE 0 0200 0.0212 mg/1 106 81-124
CHLOROFORM 0 . 0200 0 . 0244 mg/1 122 75-138
DIBROMOCHLOROMETHANE 0.0200 0 0215 mg/1 107 82-137
TETRACHLOROETHENE 0.0200 0 .0210 mg/1 105 71-120
TOLUENE o. 0200 0. 0211 mg/1 106 81-121
TRICHLOROETHENE 0.0200 0 0222 mg/1 111 ?6-120
VINYL CHLORIDE o. 0200 0 0180 mg/1 90 51-138
Davis & Floyd, Inc. I PO Drawer 428 ) Greenwood, SC 19648 I 816 E. Durst Avenue I Greenwood, SC 2%49 I (8641 2'.:9-4413 I Fax W64) 229-7119
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Di\:VIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Cenification Number: 25
Project Number: 61621.01
Report Date
Page 51 of as
April 18, 2005
Report ID: AC1040
QC Batch Report -Batch Sample List
WorkGroup WG40428 Matrix GW/ChemW
□e._scription: V0/8260/TCL RDL of 1 Prep Method
Analtyical Method: SW846 8260B
PREP ANALYTICAL
Sample ID Client ID Run# Date Time Date Time Analyst
L05021803-01 DUP-1 1 02/24/2005 0837 PAP
LOS021803-06 EB-01 02/24/2005 0819 PAP
L05021,8.'05-10 TRIP BLANK 02/24/2005 0743 PAP
L05022303-01 PEW-1 02/24/2005 0856 PAP
L05022303-02 PEW-3 1 02/24/2005 0915 PAP
L05022303-03 PEW-4 1 02/24/2005 0933 PAP
L050223 03-04 DUP-4 1 02/24/2005 0951 PAP
L05022303-05 TRIP BLANK-3 02/24/2005 0801 PAP
L0502240l~Ol V-23 02/24/2005 1246 PAP
L05022401-02 K-28 1 02/24/2005 1343 PAP
L05022401-03 TRIP BLANK-4 1 02/24/2005 1227 PAP
MB40428:l Method Blank 1 02/24/2005 0722 PAP
LCS40428:1 Laboratory Control Spike 1 02/24/2005 1105 PAP
MS05022303-02:40428 Matrix Spike 1 02/24/2005 1028 PAP
M8D05022303-02:40428 Matrix Spike Duplicate 02/24/2005 1047 PAP
Dilution
1
1
1
1
1
1
1
1
1
Davis & Floyrl, Inc. I PO Drawer 42H I Greenwood, SC 29648 I fil h E. Ours! Avenue I Creenwonr!, SC 19649 I (864) 129-4413 I Fax (864) 229-7119
LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Cenijication Number: 25
Project Number: 61621.01
Report Date April 18, 2005
Page 52 of 88 Report ID: AC1040
QC Batch Report -Surrogates % Recovery
WorkGroup: WG40428 Matrix GW/ChemW
Prep Method
Analtyical Method: SW846 82608
L05021803-01 02/24/2005 0837 110 102 97
LOS021803-06 02/24/2005 0819 107 103 98
LOS021805-10 02/24/2005 0743 102 103 97
L05022303-01 02/24/2005 0856 109 104 95
LOS022303-02 02/24/2005 0915 111 104 96
L05022J03-03 02/24/2005 0933 109 104 97
L05022303-04 02/24/2005 0951 109 104 96
L05022303-0S 02/24/2005 0801 102 100 95
L05022401-0l 02/24/2005 1246 103 105 95
105022401-02 02/24/2005 1343 93 101 96
L05022401-03 02/24/2005 1227 116 107 97
MB40428:l 02/24/2005 0722 101 101 97
LCS40428:l 02/24/2005 1105 115 106 96
MS05022303-02:40428 02/24/2005 1028 114 106 95
MSD05022303-02:4042B 02/24/2005 1047 114 105 96
DCE 1,2-DICHLOROETHANE-D4
BFB BROMOFLUOROBENZENE
TOL TOLUENE-DB
Davis & Floyd, Inc. I PO Drawer 428 / Greenwood, SC 29648 I 816 F.. Durst Avenue I Greenwood, SC 2%49 I (864) 229-441 J I Fax {B64) 229-7119
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DAYIS
FLMD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
QC Batch Report -Method Blanks
WorkGroup, WG40t28
Bl,ank MB40428:1
Parameter Result Qual
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE ' 0 0010
1,1,2,2-TETRACHLOROETHANE ' 0 0010
1, 1, 2-.TRICHLOROETHANE ' 0 .0010
1,1-DICHLOROETHANE ' 0 .0010
1,1-DICHLOROETHENE ' 0. 0010
1,2-DICHLOROETHANE ' . 0 0010
1,2-DICHLOROPROPANE ' 0 0010
2-BUTANONE ' 0.0050
2-HEXANONE ' 0.0050
4-METHYL-2-PENTANONE ' 0.0050
ACETONE ' 0.0050
BENZENE ' 0.0010
BROMODICHLOROMETHANE ' 0.0010
BROMOFORM ' 0.0010
BROMOMETHANE ' 0.0010
CARBON DISULFIDE ' 0.0010
CARBON TETRACHLORIDE ' 0.0010
CHLOROBENZENE ' 0.0010
CHLOROETHANE ' 0.0010
CHLOROFORM ' 0.0010
CHLOROMETHANE ' 0 0010
CIS-1,2-DICHLOROETHENE ' o. 0010
CIS-1,3-DICHLOROPROPENE ' 0 .0010
DIBROMOCHLOROMETHANE ' 0. 0010
ETHYLBENZENE ' 0 0010
METHYLENE CHLORIDE ' 0.0010
STYRENE ' 0.0010
TETRACHLOROETHENE ' 0.0010
TOLUENE ' 0 .0010
TRANS-1,2-DICHLOROETHENE ' 0.0010
TRANS-1,3-DICHLOROPROPENE ' 0.0010
TRICHLOROETHENE ' 0.0010
VINYL ACETATE ' 0.0010
VINYL CHLORIDE ' 0.0010
XYLENE (TOTAL) ' 0.0020
NC Cenijication Number: 25
Project Number: 61621.01
Report Date April 18, 2005
Page 53 of 88 Report ID: AC1040
Matrix: GW/Chemw
RDL units Analyst Date Time
0.0010 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0.0050 mg/1 PAP 02/24/2005 0722
0.0050 mg/1 PAP 02/24/2005 0722
0.0050 mg/1 PAP 02/24/2005 0722
0.0050 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0 0010 mg/1 PAP 02/24/2005 0722
0 0010 mg/1 PAP 02/24/2005 0722
0 .0010 mg/1 PAP 02/24/2005 0722
0. 0010 mg/1 PAP 02/24/2005 0722
0. 0010 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0. 0010 mg/1 PAP 02/24/2005 0722
0 .0010 mg/1 PAP 02/24/2005 0722
0. 0010 mg/1 PAP 02/24/2005 0722
0. 0010 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0.0010 mg/1 PAP 02/24/2005 0722
0 0010 mg/1 PAP 02/24/2005 0722
0.0020 mg/1 PAP 02/24/2005 0722
I D,wis ,I(.: Floyd, Inc. I PO Drawer 42/-1 I Greenwurnl, SC 291)4/l I 816 E. Durst Ave1111e I Greenwood, SC 29(i49 I (B64) 221)-4413 I Fax (8fi4) 229-7"119
D:\YIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA, LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Cenification Number: 25
Project Number: 61621.01
Report Date
Page 54 of 88
April 18, 2005
Report ID: AC1040
QC Batch Report -Matrix Spikes and Duplicates
WorkGroup: WG40428
MS05022303-02:40428
MSD05022303-.02: 40428
1,1,1-TRICHLOROETHANE 0 .osoo
1,1,2-TRICHLOROETHANE 0 . 0500
1,1-DICHLOROETHENE 0.0500
1,2-DitjH . .OROETHANE 0.0500
1,2-DICHLOROPROPANE 0.0500
2.-BUTANONE 0.0500
BENZENE 0 .0500
CARBON TETRACHLORIDE 0. 0500
CHLOROBENZENE 0.0500
CHLOROFORM 0.0500
DIBROMOCHLOROMETHANE 0 -0500
TETRACHLOROETHENE o. 0500
TOLUENE 0. 0500
TRICHLOROETHENE 0.0500
VINYL CHLORIDE 0.0500
1,1,1-TRICHLOROETHANE 0. 0500
1,1,2-TRICHLOROETHANE 0 .0500
1,1-DICHLOROETHENE 0. 0500
1,2-DICHLOROETHANE 0.0500
1,2-DICHLOROPROPANE 0.0500
2-BUTANONE 0.0500
BENZENE 0 .0500
CARBON TETRACHLORIDE 0. 0500
CHLOROBENZENE 0 .0500
CHLOROFORM 0. 0500
DIBROMOCHLOROMETHANE 0 .0500
TETRACHLOROETHENE 0.0500
TOLUENE 0 .0500
TRICHLOROETHENE o. 0500
VINYL CHLORIDE 0 . 0500
NOTB: MS/MSD \ recoveries are not evaluated if the
Matrix GW/Chemw
Prep Method
Analtyical Method: SW846 82608
< 0.00100 0 .0555 mg/1 111 88-124
< 0.00100 0 .0474 mg/1 95 88-128
'0. 00100 0 . 0538 mg/1 108 71-130
' 0 . 00100 0 . 0565 mg/1 113 78-143
' 0 . 00100 o . 0463 mg/1 93 91-118
' 0 .00500 0.0444 mg/1 89 28-199
' 0 .00100 0.0507 mg/1 101 77-123
<.0 .00100 0.0574 mg/1 115 63-135
< 0.00100 0.0514 mg/1 103 78-123
< 0.00100 0.0564 mg/1 113 75-135
< 0.00100 0.0557 mg/1 111 88-133
' 0.00100 0.0516 mg/1 103 69-123
< 0.00100 0.0501 mg/1 100 85-117
' 0 .00100 0.0509 mg/1 102 75-121
' 0 .00100 0.0400 mg/1 BO 47-136
0.0547 mg/1 109 1 15 88-124
0. 04 92 mg/1 98 ' 17 88-128
o. 0511 mg/1 102 5 17 71-130
0 .0560 mg/1 112 1 20 78-143
0 .0460 mg/1 92 1 14 91-118
0.0427 mg/1 85 ' 31 28-199
0.0510 mg/1 102 17 77-123
0.0579 mg/1 116 1 20 63-135
0.0506 mg/1 101 l 17 78-123
0.0557 mg/1 111 1 17 75-135
0 . 0561 mg/1 112 15 88-133
0 .0513 mg/1 103 0 17 69-123
0. 0504 mg/1 101 15 85-117
0 . 0517 mg/1 103 2 17 75-121
0.0404 mg/1 81 1 19 47-136
sample concentration is greater than four times the spike added.
Davis & Floyd, Inc. I PO Dr:1wer 428 I Creenwuud, SC 29(i48 I 81 (1 E. Durst Avcmue I Cret:nwood, SC 29649 I (/l64) 22~-441 J I fax (H64) 220-7119
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D~IS
FLMD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Cenijication Number: 25
Project Number: 61621.01
Report Date
Page 55 of 88
April 18, 2005
Report ID: AC1040
QC Batch Report -Laboratory Control Standards and Duplicates
WorkGroup: WG40428 Matrix· GW/ChemW
LCS LCS40428:l Prep Method
Analtyical Method: SW846 82608
1,1,1-TRICHLOROETHANE 0.0200 0.0231 mg/1 116 79-127
1,1,2-TRICHLOROETHANE 0.0200 0.0217 mg/1 108 B3-143
1,1-DICHLOROETHENE 0.0200 0.0220 mg/1 110 63-141
1, 2-DI,CHI..OROETHANE 0.0200 0.0250 mg/1 125 79-147
1,2-DICHLOROPROPANE 0.0200 0.0189 mg/1 95 86-130
2-BUTANONE 0.0200 0.0198 mg/1 99 52-190
BENZENE 0.0200 0. 0216 mg/1 108 7B-123
CARBON TETRACHLORIDE 0.0200 0.0248 mg/1 124 58-132
CHLOROBENZENE 0 .0200 0 0218 mg/1 109 81-124
CHLOROFORM 0.0200 0. 0242 mg/1 121 75-138
DIBROMOCHLOROMETHANE 0. 02 00 0 0240 mg/1 120 82-13 7
TETRACHLOROETHENE 0.0200 0. 0220 mg/1 110 71-120
TOLUENE 0 . 0200 0 0217 mg/1 109 81-121
TRICHLOROETHENE o. 0200 0.0215 mg/1 108 76-120
VINYL CHLORIDE o. 0200 0. 01 72 mg/1 86 51-138
Davis & rloyd, Inc. I PO Drawer 428 I Creenwood, SC 296..J.a I 8 ! h E. Dur~! Avenue I Greenwouc!, SC 29649 I (H64) 229-44 1 J I F,1x (864) 229-71 ! 9
Sample ID
L05022812-01
L05022812-0l
MB4048,7·: 1
LCS40487: 1
MS05022810-04
LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Cenification Number: 25
Project Number: 61621.01
Report Date
Page 56 of 88
April 18, 2005
Report ID: AC1040
QC Batch Report -Batch Sample List
WorkGroup WG40487 Matrix GW/ChemW
D~scription: vo/8260/TCL Prep Method
Analtyical Method: SW846 8260B
PREP ANALYTICAL
Client IC Run# Date Time Date Time Analyst
FB-01 1 03/03/2005 1216 PAP
FB-01 2 03/03/2005 1216 PAP
Method Blank 1 03/03/2005 1119 PAP
Laboratory Control Spike 03/03/2005 1748 PAP
:40487 Matrix Spike 1 03/03/2005 1331 PAP
Dilution
1
1
MSD05022810-04:40487 Matrix Spike Duplicate 1 03/03/2005 1349 PAP
Davis & F!oyd, Inc. I PO Drawer 42H I Greenwood, SC 2%48 I 816 E. Durst Avenue I Creenwood, SC 29649 I {1364) 12~-44 ! 3 I fax (H64) 229-7119
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DAYIS
FLMD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Certification Number: 25
Project Number: 61621.01
Report Date April 18, 2005
Page 57 of 88 Report ID: AC1040
QC Batch Report -Surrogates % Recovery
WorkGroup: WG40487 Matrix GW/Chemw
Prep Method
Analtyical Method: SW846 82608
LOS022812-0l 03/03/2005 1216 93 96 98
L0502281~-01 03/03/2005 1216 93
M8404S7,! i 03/03/2005 1119 95 96 98
LCS40487:l 03/03/2005 l "48 108 96 97
MS05022810-04:40487 03/03/2005 1331 112 100 97
MSD05022810-04:40487 03/03/2005 1349 116 100 98
DCE l,2-DICHLOROETHANE-04
BFB BROMOFLUOROBENZENE
TOL TOLUENE-DB
I Davis 8, Floyd, Inc. / PO Drawer 428 I Greenwood, SC 29648 I 81 fi I::. Durst Avenue I Greenwood, SC 29fi49 I {864} 229-4413 I Fax (864) 229-7119
Dl\VIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
QC Batch Report -Method Blanks
WorkGroup: WG40487
Bl~nk MB40487: l
Paramoter Result Qual
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE ' 1.0
1,1,2,2-TETRACHLOROETHANE ' 1.0
1,1,2-TRICHLOROETHANE ' 1.0
1,1-DICHLOROETHANE ' 1. 0
1,1-DICHLOROETHENE ' 1 .o
1,2-DICHLOROETHANE ' 1 0
1,2-DICHLOROPROPANE ' 1.0
2-BUTANONE ' 5 .o
2-HEXANONE ' 5.0
4-METHYL-2-PENTANONE ' 5.0
ACETONE ' 5.0
BENZENE ' 1.0
BROMODICHLOROMETHAN'E ' 1 .o
BROMOFORM ' 1.0
BROMOMETHAN'E ' 1.0
CARBON DISULFIDE ' 1.0
CARBON TETRACHLORIDE ' .o
CHLOROBENZENE ' 1.0
CHLO RO ETHANE ' 1.0
CHLOROFORM ' 1.0
CHLOROMETHANE ' 1.0
CIS-1,2-DICHLOROETHENE ' 1.0
CIS-1,3-DICHLOROPROPENE ' .0
DIBROMOCHLOROMETHANE ' 1 .o
ETHYLBENZENE ' 1 .o
METHYLENE CHLORIDE ' 1.0
STYRENE ' 1.0
TETRACHLOROETHENE ' 1.0
TOLUENE ' 1.0
TRANS-1,2-DICHLOROETHENE ' 1.0
TRANS-1,3-DICHLOROPROPENE ' 1.0
TRICHLOROETHENE ' 1 0
VINYL ACETATE ' 1.0
VINYL CHLORIDE ' .0
XYLENE (TOTAL) ' ' .0
NC Certification Number: 25
Project Number: 61621.01
Report Date April 18, 2005
Page 58 of 88 Report ID, AC1040
Matrix: GW/Chemw
RDL Units Analyst Date Tima
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
5.0 ug/1 PAP 03/03/2005 1119
5.0 ug/1 PAP 03/03/2005 1119
5.0 ug/1 PAP 03/03/2005 1119
5.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
. 0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
1. 0 ug/1 PAP 03/03/2005 1119
. 0 ug/1 PAP 03/03/2005 1119
1 0 ug/1 PAP 03/03/2005 1119
.0 ug/1 PAP 03/03/2005 1119
1.0 ug/1 PAP 03/03/2005 1119
2.0 ug/1 PAP 03/03/2005 1119
Dilvl!:i & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2%48 / 81 r, E. Durst Avenue I Greenwood, SC 29049 I (864) ~29-44 lJ I Fax (864) 229-7119
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DAcYIS
FLWD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 59 of 88
April 18, 2005
Report ID: AC1040
QC Batch Report -Matrix Spikes and Duplicates
WorkGroup: WG40487 Matrix GW/ChemW
MS{MSD MS0S022810-04:40487 Prep Method
MSD05022810-04:40487 Analtyical Method: SW846 82608
1,1,1-TRICHLOROETHANE so. 00 < 5. 00 56.42 ug/1 113 88-124
1,1,2-TRICHLOROETHANE 50.00 < 5. 00 46.35 ug/1 97 88-128
1,1-DICHLOROETHENE 50.00 < 5.00 49. 72 ug/1 99 71-130
1, 2-DI,CHLOROE'THANE 50.00 < 5. 00 55.40 ug/1 111 78-143
1,2-DICHLOROPROPANE 50.00 < 5.00 49. 31 ug/1 99 91-118
2-BUTANONE so.co < 10.00 56.52 ug/1 113 28-199
BENZENE 50.00 < 5.00 46.59 ug/1 93 77-123
CARBON TETRACHLORIDE 50.00 < 5.00 57.96 ug/1 116 63-135
CHLOROBENZENE SO.DO < 5.00 47.90 ug/1 96 78-123
CHLOROFORM 50.00 < 5.00 51. 43 ug/1 103 75-135
DIBROMOCHLOROMETHANE 50.00 < 5. 00 57. 33 ug/1 115 88-133
TETRACHLOROETHENE 50.00 < 5. 00 52. 91 ug/1 106 69-123
TOLUENE 50. 00 < 5 .00 48.66 ug/1 97 85-117
TRICHLOROETHENE 50. 00 < 5. 00 50.22 ug/1 100 75-121
VINYL CHLORIDE 50.00 < 10. 00 55.40 ug/1 111 47-136
1,1,1-TRICHLOROETHANE 50.00 55. 41 ug/1 111 2 15 88-124
1,1,2-TRICHLOROETHANE 50.00 48.64 ug/1 97 l 17 88-128
1,1-DICHLOROETHENE 50.00 46. 79 ug/1 94 6 17 71-13 0
1,2-DICHLOROETHANE 50.00 56. 19 ug/1 112 l 20 78-143
1,2-DICHLOROPROPANE 50.00 48. 49 ug/1 97 2 14 91-118
2-BUTANONE 50.00 61. 34 ug/1 123 a 31 28-199
BENZENE 50.00 45. 79 ug/1 92 2 17 77-123
CARBON TETRACHLORIDE 50.00 56 .23 ug/1 112 3 20 63-135
CHLOROBENZENE 50.00 47.08 ug/1 94 2 17 78-123
CHLOROFORM 50.00 so. 76 ug/1 102 l 17 75-135
DIBROMOCHLOROMETHANE 50.00 58.42 ug/1 117 2 15 88-133
TETRACHLOROETHENE 50.00 51. 90 ug/1 104 2 17 69-123
TOLUENE 50.00 47. 36 ug/1 95 3 15 85-117
TRICHLOROETHENE so.oo 48. 72 ug/1 97 3 17 75-121
VINYL CHLORIDE 50.00 52. 64 ug/1 105 5 19 47-136
NOTE1 MS/MSD \ recoveries are not evaluated if the sample concentration is greater than four times the spike added.
Davis & Floyd, Inc. I PO Drawer 428 I Creenwood, SC 29fi48 j 81 I) E. Durst Avenue I Greenwood, SC 20(149 I (864) 229-4413 I Fax (864) 229-7119
' ,
Df\YIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA, LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Cenijication Number: 25
Project Number: 61621.01
Report Date
Page 60 of 88
April 18, 2005
Report ID: AC1040
QC Batch Report -Laboratory Control Standards and Duplicates
WorkGroup: WG40487 Matrix GW/Chemw
LCS LCS40487:1 Prep Method
Analtyical Method: SW846 82608
1,1,1-TRICHLOROETHANE 20.00 20. 03 ug/1 100 79-127
1,1,2-TRICHLOROETHANE 20.00 20. 35 ug/1 102 83-143
1,1-DICH~ROETHENE 20.00 20.01 ug/1 100 63-141
1,2-DICHi.oROETHANE 20.00 22.57 ug/1 113 79-147
1, 2-.DICHLOROPROPANE 20.00 19.57 ug/1 98 86-130
2.-BUTANONE 20.00 22.01 ug/1 110 52-190
BENZENE 20.00 19. 55 ug/1 98 78-123
CARBON TETRACHLORIDE 20.00 20. 22 ug/1 101 58-132
CHLOROBENZENE 20.00 19. 89 ug/1 99 81-124
CHLOROFORM 20.00 20.82 ug/1 104 75-138
DIBROMOCHLOROMETHANE 20.00 21.27 ug/1 106 82-13 7
TETRACHLOROETHENE 20.00 20. 55 ug/1 103 71-12 0
TOLUENE 20.00 19 93 ug/1 100 81-121
TRICHLOROETHENE 20.00 19. 87 ug/1 99 76-120
VINYL CHLORIDE 20.00 20 51 ug/1 103 51-138
Davis & Floyd, Inc. I PO Drawer 42H I Greenwood, SC 2%48 I 816 E. Durst Avenue ! Gr(!Cnwood, SC 2%49 / (86.J) ~29-4413 I Fax (864) 229-7119
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D~IS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Cenijication Number: 25
Project Number: 61621.01
Report Date
Page 61 of ea
April 18, 2005
Report ID: AC1040
QC Batch Report -Batch Sample List
WorkGroup WG40388
D~scription: SV/8270/BNA/TCL SV/DOW
Sample ID Client ID Run#
L05022007-02 F-55 1
L0502200_7-02 F-55 2
MB4038_8·: 1 Method Blank 1
LCS40388:1 Laboratory Control Spike 1
MS05022007-02 :40388 Matrix Spike 1
MSD05022007-02:40388 Matrix Spike Duplicate 1
Matrix
Prep Method
GW/ChemW
SW846 3510C
Analtyical Method: SW846 8270C
PREP ANALYTICAL
Date Time Date Time
02/22/2005 0800 03/01/2005 1845
02/22/2005 0800 03/02/2005 1256
02/22/2005 0800 03/01/2005 1235
02/22/2005 0600 03/01/2005 1316
02/22/2005 0800 03/01/2005 1925
02/22/2005 0800 03/01/2005 2008
Analyst
JRN
JRN
JRN
JRN
JRN
JRN
Dilution
10
1
1
I Davis & rluyd, Inc. I PO Drawer 428 I Creenwood, SC 21JM8 I 6161:. Dursl ,-\venue I Greenwood, SC 2964'.I I (8(>•!) 22()-4413 I Fax (864) 229-7119
DAYIS
FLMD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Cenification Number: 25
Project Number: 61621.0l
Report Date April 18, 2005
Page 62 of 88 Report ID: AC1040
QC Batch Report -Surrogates % Recovery
WorkGroup: WG40388
L05022007-02 03/01/2005 1845
M840388: ~ 03/01/2005 1235
LCS40388:1 03/01/2005 1316
MS05022007-02 :40388 03/01/2005 1925
MSD05022007-02:40388 03/01/2005 2008
TBP 2,4,6-TRIBROMOPHENOL
FBP 2-FLUOROBIPHENYL
2FP 2-FLUOROPHENOL
NBZ NITROBENZENE-D5
PHL PHENOL-OS
TPH TERPHENYL-D14
91 111
74 77
78 82
90 104
90 105
Matrix
Prep Method
GW/ChemW
SW846 3510C
Analtyical Method: SW846 8270C
81 74 1
73 98 61
77 97 61 ,o 48 0
90 29 2
64
87
90
55
56
0;1vis & Floyd, Inc. I PO Drawer 42B I Greenwoorl, SC 2~1648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (/3(,,!) 229-44B I r-,1x (8(;4) 229-71 I~
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem carter
QC Batch Report -Method Blanks
WorkGroup: WG40388
Blfnk MB40388:l
Parameter Result Qual
Semi volatile Organics
SW846 8270C
1,2,4-TRICHLOROBENZENE ' 0. 010
1,2-DICHLOROBENZENE ' 0. 010
1, 3-DI,CHLOROBENZENE ' 0.010
1,4-DICHLOROBENZENE ' 0. 010
2,4,5-TRICHLOROPHENOL ' 0.010
2,4,6-TRICHLOROPHENOL ' 0.010
2,4-DICHLOROPHENOL ' 0. 010
2,4-DIMETHYLPHENOL ' 0.010
2,4-DINITROPHENOL ' 0.025
2,4-DINITROTOLUENE ' 0.010
2,6-DINITROTOLUENE ' 0.010
2-CHLORONAPHTHALENE ' 0.010
2-CHLOROPHENOL ' o. 010
2-METHYL-4,6-DINITROPHENOL ' o. 025
2-METHYLNAPHTHALENE ' o. 010
2-METHYLPHENOL ' o. 010
2-NITROANILINE ' o. 010
2-NITROPHENOL ' 0. 010
3,3'-DICHLOROBENZIDINE ' 0 .010
3-NITROANILINE ' 0. 010
4-BROMOPHENYL PHENYL ETHER ' 0.010
4-CHLOR0-3-METHYLPHENOL ' 0.010
4-CHLOROANILINE ' 0.010
4-CHLOROPHENYL PHENYL ETHER ' 0.010
4 -METHYLPHENOL ' 0. 010
4-NITROANILINE ' ~-010
4-NITROPHENOL ' 0.025
ACENAPHTHENE ' 0.010
ACENAPHTHYLENE ' 0.010
ANTHRACENE ' 0.010
BENZO(A)ANTHRACENE ' 0.010
BENZO(A)PYRENE ' 0.010
BENZO{B)FLUORANTHENE ' 0.010
BENZO{G,H,I)PERYLENE ' 0.010
BENZO(K)FLUORANTHENE ' 0. 010
BENZOIC ACID ' 0. 050
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 63 of 88
Matrix: GW/ChemW
RDL Units
0.010 mg/1
0 .010 mg/1
0 .010 mg/1
0 .010 mg/1
0 .010 mg/1
0. 010 mg/1
0 .010 mg/1
0 .010 mg/1
0 .025 mg/1
0. 010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0.025 mg/1
0. 010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0. 010 mg/1
0.010 mg/1
0.010 mg/1
0,010 mg/1
o. 010 mg/1
0 010 mg/1
0. 010 mg/1
0 .025 mg/1
0 .010 mg/1
0 .010 mg/1
0.010 mg/1
0 .010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0.050 mg/1
April 18, 2005
Report ID: AC1040
Analyst Date
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
Time
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
I Davis & Floyd, Inc. I PO Drawer 41.H I Creenwood, SC 2964B I H 16 I:. Durst Avenue I Greenwood, .SC 2%4(J I (8G4) :!.:!.9-4413 I Fax (864) 229-7119
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
QC Batch Report-Method Blanks
WorkGroup: WG40388
Blfnk MB40388:l
Parameter Result Qual
BENZYL ALCOHOL ' 0.010
BIS(2-CHLOROETHOXY)METHANE ' 0.010
BIS(2-CHLOROETHYL)ETHER ' 0.010
BIS(2-CHLOROISOPR0PYL)ETHER ' 0.010
BIS(2-~HYLHEXYL)PHTHALATE ' 0.010
BUTYL BENZYL PHTHALATE ' 0. 010
CHRYSENE ' 0.010
D1-N-BUTYL PHTHALATE ' 0.010
DI-N-OCTYL PHTHALATE ' 0.010
DIBENZ(A,H)ANTHRACENE ' 0. 010
DIBENZOFURAN ' 0.010
DIETHYL PHTHALATE ' 0.010
DIMETHYL PHTHALATE ' 0. 010
FLUORANTHENE ' 0.010
FLUORENE ' 0.010
HEXACHLOROBENZENE ' 0.010
HEXACHLOROBUTADIENE ' 0.010
HEXACHLOROCYCLOPENTADIENE ' 0.010
HEXACHLOROETHANE ' 0. 010
INDENO(l,2,3-CD)PYRENE ' 0.010
ISOPHORONE ' 0.010
N-NITROSODI-N-PROPYLAMINE ' 0. 010
N-NITROSODIPHENYLAMINE ' 0.010
NAPHTHALENE ' 0.010
NI TROBENZENE ' 0. 010
PENTACHLOROPHENOL ' 0.025
PHENANTHRENE ' 0.010
PHENOL ' o .. 010
PYRENE ' 0.010
SW846 8270C DOWI'HERM
1,1'-BIPHENYL ' 0. 010
BIPHENYL ETHER ' 0.010
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 64 of 88
Matrix: GW/ChemW
RDL Units
0.010 mg/1
0. 010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0. 010 mg/1
0. 010 mg/1
0. 010 mg/1
0. 010 mg/1
0. 010 mg/1
0.010 mg/1
0. 010 mg/1
0.010 mg/1
0 010 mg/1
0 010 mg/1
0. 010 mg/1
o. 010 mg/1
0 010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0.025 mg/1
0.010 mg/1
0. 010 mg/1
0. 010 mg/1
0 010 mg/1
0.010 mg/1
April 18, 2005
Report ID: AC1040
Analyst Date
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
Time
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
Davis &-floyrl, Inc. I PO DrJwer 428 Creenwood, SC 29648 I 816 E. Durst Avenue I Creenwund, SC 29649 I (B64) 229-441 J I F,ix (864) L.29-7 l 19
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DAYIS
FLbYD
Client
Contact
LABORATORY ANALYSIS REPORT
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pcm Carter
NC Certification Number: 25
Project Number: 61621.01
Report ~ate
Page 65 of 88
April 18, 2005
Report ID: AC1040
QC Batch Report -Method Blanks
WorkGroup: WG40388 Matrix: GW/ChemW
Blank MB403881l
Prep Procedure Method Analyst Prep Date
Analytical Prep Procedures:
DOWTHERM SW846 35008 DBC 02/22/2005 0800
82?0 SVOC PREP SW846 3510C DBC 02/22/2005 0800
I Davis S, Floycl, Inc. I 1-'0 Drawer 42H I Creenwnl)d, SC 2%4B I 816 E. Durs! Avenue I Gree11wuod, SC 2%•i9 I (Hfi ... +J 229-441 :I I F.ix (1364) 229-71 19
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Cenijication Number: 25
Project Number: 61621.01
Report Date
Page 66 of 88
April 18, 2005
Report ID: AC1040
QC Batch Report -Matrix Spikes and Duplicates
WorkGroup: WG40388
M1/MSD
1,2,4-TRICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4-DINITROTOLUENE
2 -CHLO,RONAPHTHALENE
2-CHLOROPHENOL
2-NITROPHENOL
4 -BROMOPHENYL PHENYL ETHER
4-CHLOR0-3-METHYLPHENOL
4-NITROPHENOL
ACENAPHTHENE
DI-N-OCTYL PHTHALATE
N-NITROSODI-N-PROPYLAMINE
PENTACHLOROPHENOL
PHENOL
PYRENE
1,2,4-TRICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-NITROPHENOL
4 -BROMOPHENYL PHENYL ETHER
4-CHLOR0-3-METHYLPHENOL
4 -NI TROPHENOL
ACENAPHTHENE
DI-N-OCTYL PHTHALATE
N-NITROSODI-N-PROPYLAMINE
PENTACHLOROPHENOL
PHENOL
PYRENE
MS05022007-02:40388
MSD05022007-02:40388
0.0500
0 .0500
0 . 0500
0. 0500
0 .0750
0.0750
0.0500
0.0750
0.0750
0.0500
0.0500
0.0500
0.0750
0.0750
0.0500
0 .0500
0 .0500
0 .0500
0 .0500
0.0750
0.0750
0.0500
0.0750
0.0750
o.osoo
0.0500
0. 0500
0.0750
0.0750
0.0500
NOTB1 MS/MSD t recoveries are not evaluated if the
< 0 .0100
< 0 . 0100
< o . 0100
< 0 .0100
< 0 .0100
< 0.0100
< 0.0100
< 0.0100
< 0.0250
< 0.0100
< 0.0100
< 0.0100
< 0 . 0250
0 .340
< o. 0100
0.0189
0. 0392
0.0100
0.0100
0.0808
0.0100
0.0351
0.110
0. 0592
0.0100
0.0195
0 .155
0.0521
0. 433
0.0409
Matrix
Prep Method
GW/ChemW
SW846 3510C
Analtyical Method: SW846 8270C
0.0235 mg/1 47
0.0309 mg/1 62
0.0318 mg/1 64
0 .0100 mg/1 5
0 .0764 mg/1 102
0. 0100 mg/1 3
0 . 0341 mg/1 68
0. 0906 mg/1 121
0.0250 mg/1 7
0.0100 mg/1 15
0.0190 mg/1 38
0.165 mg/1 81
0.0556 mg/1 74
0 .418 mg/1 105
0.0388 mg/1 78
mg/1 38 22
mg/1 78 ,.
mg/1 0 200
mg/1 • 18
mg/1 108 6
mg/1 0 200
mg/1 70 3
mg/1 147 19
mg/1 79 166
mg/1 0 200
mg/1 39 3
mg/1 62 6
mg/1 69 7
mg/1 125 3
mg/1 82 5
sample concentration is greater than four times
33-92
30-86
45-107
70-130
34-95
70-130
70-130
35-110
16-88
41-107
70-130
36-106
32-126
4-83
51-132
30 33-92
20 30-86
22 45-107
20 70-130
29 34-95
20 70-130
20 70-130
22 35-110
28 16-88
26 41-107
20 70-130
22 36-106
38 32-126
28 4-83
24 51-132
the spike added.
D;:wis & Floyd, Inc. I PO Drawer 42f:I I Grr!enwond, SC 29(AH I I.I! r) E. Durst Avenut~ I Greenwood, SC 2%49 I (H(14) 229-4413 I Fax (Bti4) 229-71 19
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DAYIS
FL6YD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Cenification Number: 25
Project Number: 61621.01
Report Date
Page 67 of 88
April 18, 2005
Report ID: AC1040
QC Batch Report -Laboratory Control Standards and Duplicates
WorkGroup: WG40388
Lq, LCS40388:1
1,2,4-TRICHLOROBEN~ENE 0.0500
1,4-DICHLOROBENZENE 0.0500
2,4-DINI!ROTOLUENE 0.0500
2-CHLORONAPHTHALENE 0.0500
2-CHLOROPHENOL 0.0750
2-NITROPHENOL 0.0750
4-BROMOPHENYL PHENYL ETHER 0.0500
4-CHLOR0-3-METHYLPHENOL 0.0750
4-NITROPHENOL 0.0750
ACENAPHTHENE 0.0500
DI-N-OCTYL PHTHALATE o. 0500
N-NITROSODI-N-PROPYLAMINE 0. 0500
PENTACHLOROPHENOL 0 0750
PHENOL 0. 0750
PYRENE 0.0500
0.0333
0.0308
0. 0455
0.0374
0. 0547
0.0612
0.0383
0.0661
0.0435
o. 0410
0 .0565
0 . 0456
0 . 0339
0.0426
0.0459
Matrix
Prep Method
GW/ChemW
SW846 3510C
Analtyical Method: SW846 8270C
mg/1 67 30-91
mg/1 62 29-83
mg/1 91 46-108
mg/1 75 60-118
mg/1 73 29-106
rng/1 82 49-111
mg/1 77 61-111
mg/1 88 34-110
mg/1 58 4-80
mg/1 82 39-109
mg/1 113 59-111
mg/1 91 36-114
mg/1 45 20-102
mg/1 57 2-83
mg/1 92 55-126
Davis & Floyd, Inc. I PO Drawer 428 I C1eenwood, SC 29648 I H 16 E. Durst Avenue I Crcenwood, SC 2964~) I {864) 229-44 U I Fax (864) 229-7"1 19
DAYIS
FLtTYD LABORATORY ANALYSIS REPORT
Sample ID
L05022303-01
L05022303-02
LOS022,i03-03
L05022303-04
L05022812-01
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 68 of 88
April 18, 2005
Report ID: AC1040
QC Batch Report -Batch Sample List
WorkGroup WG40471
D~scription: SV/8270/BNA/TCL SV/DOW
Client ID Run#
PEW-1 1
PEW-3
PEW-4 1
DUP-4 1
FB-01 1
Matrix
Prep Method
GW/ChemW
SW846 3510C
Analtyical Method: SW846 8270C
PREP ANALYTICAL
Date Time Date Time
02/28/2005 0800 03/03/2005 1238
02/28/2005 0800 03/03/2005 1515
02/28/2005 0800 03/03/2005 1557
02/28/2005 0800 03/03/2005 1636
02/28/2005 0800 03/03/2005 1715
Analyst
JRN
JRN
JRN
JRN
JRN
Dilution
Davi:-& Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst 1\venue I Greenwood, SC 29649 I (864) 229-4413 I Fax (864) 229-71 19
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DAYIS
FLtJYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Certification Number: 25
Project Number: 61621.01
Report Date April 18, 2005
Page 69 of BB Report ID: AC1040
QC Batch Report -Surrogates % Recovery
WorkGroup: WG40471 Matrix GW/ChemW
Prep Method SW846 3510C
Analtyical Method: SW846 8270C
L05022303-01 03/03/2005 1238 45 42 36 44 29
105022303-02 03/03/2005 1515 83 84 63 83 52
L050223·o·3-03 03/03/2005 1557 80 59 46 60 39
L05022303-04 03/03/2005 1636 " 78 65 81 50
105022812-01 03/03/2005 1715 77 63 52 68 42
TBP 2,4,6-TRIBROMOPHENOL
FBP 2-FLUOROBIPHENYL
2FP 2 -FLUOROPHENOL
NBZ NITROBENZENE-D5
PHL PHENOL-OS
TPH TERPHENYL-D14
44
77
86
83
74
I Davis & Floyd, Inc. I PO Drawer 420 I Creenwond, SC 29648 I 816 E. Durst Avcmu! I Creenwoorl, SC 29fi49 I WM) 229-4413 I Fax (1164) 229-71 19
Di\YIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 70 of 88
April 18, 2005
Report ID: AC1040
QC Batch Report -Batch Sample List
WorkGroup WG40388
Dercription: SV/8270/BNA/TCL SV/DOW
Sample ID Client ID Run#
L05022007-02 F-55
L05022007-02 F-55 2
MB4038W~ 1 Method Blank 1
LCS40388:1 Laboratory Control Spike
MS05022007-02:40388 Matrix Spike 1
MSD05022007-02:40388 Matrix Spike Duplicate 1
Matrix
Prep Method
GW/Chemw
SW846 35008
Analtyical Method: SW846 8270C DOWTHERM
PREP ANALYTICAL
Date Time Date Time Analyst
02/22/2005 0800 03/01/2005 1806 JRN
02/22/2005 0800 03/01/2005 1845 JRN
02/22/2005 0800 03/01/2005 1235 JRN
02/22/2005 0800 03/01/2005 1316 JRN
02/22/2005 0800 03/01/2005 1925 JRN
02/22/2005 0800 03/01/2005 2008 JRN
Dilution
1000
1
1
1
Davis & Floyrl, Inc. I PO Drawer 428 j Greenwood, SC 29648 / 8 I 6 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-4413 I Fax (864) 229-7119
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DAYIS
FLiWD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem carter
NC Certification Number: 25
Project Number, 61621.01
Report Date
Page 71 of 88
April 18, 2005
Report ID: AC1040
QC Batch Report -Surrogates % Recovery
WorkGroup: WG40388
L05022007-02 03/01/2005
MB40388:l 03/01/2005
LCS403!38:l 03/01/2005
MS05022007-02:40388 03/01/2005
MSD05022007-02:40388 03/01/2005
FBP -2-FLUOROBIPHENYL
NOTB: *NE -Result was not evaluated.
1845 116
1235 81
1316 86
1925 •NE
2008 •NE
Matrix
Prep Method
GW/Chemw
SW846 3500B
Analtyical Method: SW846 8270C DOWTHERM
D;ivis & Floyrl, Inc. I PO Dr,1.wcr 42B I Gre1~nwood, SC 29,;,rn I 111 fi F.. Durst Ave11tll! I Gree11wnnd, SC 2%4'.J I (H64) 229-441 J I Fc1x WG4) 229~7119
DAYIS
FL(WD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
QC Batch Report-Method Blanks
workGroup: WG40388
B\ank MB403881l
Parameter Result Qual
Semi volatile Organics
SW846 8270C
1,2,4-TRICHLOROBENZENE ' 0.010
1,2-DICHµ)ROBENZENE ' 0.010
1, 3-Dl,CHLOROBENZENE ' 0.010
1,4-DICHLOROBENZENE ' 0.010
2,4,5-TRICHLOROPHENOL ' 0.010
2,4,6-TRICHLOROPHENOL ' 0.010
2,4-DICHLOROPHENOL ' 0. 010
2,4-DIMETHYLPHENOL ' 0.010
2,4-DINITROPHENOL ' 0.025
2,4-DINITROTOLUENE ' 0.010
2,6-DINITROTOLUENE ' 0. 010
2-CHLORONAPHTHALENE ' 0.010
2-CHLOROPHENOL ' 0.010
2-METHYL-4,6-DINITROPHENOL ' 0.025
2-METHYLNAPHTHALENE ' 0.010
2-METHYLPHENOL ' 0.010
2-NITROANILINE ' 0.010
2-NITROPHENOL ' 0.010
3,3'-DICHLOROBENZIDINE ' 0.010
3-NITROANILINE ' 0. 010
4-BROMOPHENYL PHENYL ETHER ' 0. 010
4-CHLOR0-3-METHYLPHENOL ' 0.010
4-CHLOROANILINE ' 0.010
4-CHLOROPHENYL PHENYL ETHER ' 0.010
4-METHYLPHENOL ' 0.010
4-NITROANILINE ' 0.010
4-NITROPHENOL ' 0.025
ACENAPHTHENE ' 0.010
ACENAPHTHYLENE ' 0.010
ANTHRACENE ' o. 010
BENZO(A)ANTHRACENE ' 0.010
BENZO(A)PYRENE ' 0.010
BENZO(B)FLUORANTHENE ' 0.010
BENZO(G,H,I)PERYLENE ' 0.010
BENZO(K)FLUORANTHENE ' 0 010
BENZOIC ACID ' 0.050
NC Cenijication Number: 25
Project Number: 61621.01
Report Date April 18, 2005
Page 72 of 88 Report ID: AC1040
Matrix: GW/ChemW
RDL Units Analyst Date Time
0.010 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
o. 010 mg/1 JRN 03/01/2005 1235
0 0l0 mg/1 JRN 03/01/2005 1235
0 .010 mg/1 JRN 03/01/2005 1235
0 .010 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
0.025 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
0.025 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
0. 010 mg/1 JRN 03/01/2005 1235
0. 010 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
0.025 mg/1 JRN 03/01/2005 1235
0. 010 mg/1 JRN 03/01/2005 1235
0 .010 mg/1 JRN 03/01/2005 1235
0. 010 mg/1 JRN 03/01/2005 1235
0. 0l0 mg/1 JRN 03/01/2005 1235
o. 010 mg/1 JRN 03/01/2005 1235
o. 010 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
0.010 mg/1 JRN 03/01/2005 1235
0.050 mg/1 JRN 03/01/2005 1235
Davis & Floyd, Inc. I PO Draw1:r 42H I Greenwood, SC 29648 I 8 l 6 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-4413 I F<1x (864) 229-7119
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DA[IS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem carter
QC Batch Report-Method Blanks
WorkGroup: WG-10388
Bl~ank MB403881l
Parameter Result Qual
BENZYL ALCOHOL ' 0.010
818(2-CHLOROETHOXY)METHANE ' 0.010
818(2-CHLOROETHYL)ETHER ' 0.010
818(2-CHLOROISOPROPYL)ETHER ' 0.010
BIS (2-_E1°HYLHEXYL) PHTHALATE ' 0.010
BUTYL BENZYL PHTHALATE ' 0.010
CHRYSENE ' 0.010
DI-N-BUTYL PHTHALATE ' 0.010
DI-N-OCTYL PHTHALATE ' 0.010
DIBENZ(A,H)ANTHRACENE ' 0.010
DIBENZOFURAN ' 0.010
DIETHYL PHTHALATE ' 0.010
DIMETHYL PHTHALATE ' 0.010
FLUORANTHENE ' 0.010
FLUORENE ' 0.010
HEXACHLOROBENZENE ' 0.010
HEXACHLOROBUTADIENE ' 0 .010
HEXACHLOROCYCLOPENTADIENE ' 0. 010
HEXACHLOROETHANE ' 0 .010
INDENO(l,2,3-CD)PYRENE ' 0. 010
ISOPHORONE ' 0.010
N-NITROSOOI-N-PROPYLAMINE ' 0.010
N-NITROSODIPHENYLAMINE ' 0.010
NAPHTHALENE ' 0.010
NITROBENZENE ' 0.010
PENTACHLOROPHENOL ' 0.025
PHENANTHRENE ' 0.010
PHENOL ' 0.010
PYRENE ' 0.010
SW846 8270C DOWTHERM
1,1'-BIPHENYL ' 0 .010
BIPHENYL ETHER ' 0.010
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 73 of BB
Matrix: GW/Chemw
RDL Units
0. 010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0 010 mg/1
0.010 mg/1
0. 010 mg/1
0. 010 mg/1
0. 010 mg/1
0.010 mg/1
0. 010 mg/1
0.010 mg/1
0. 010 mg/1
0.010 mg/1
0. 010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0.010 mg/1
0. 010 mg/1
0. 025 rng/1
0.010 mg/1
0. 010 mg/1
0. 010 mg/1
0.010 mg/1
0.010 mg/1
April 18, 2005
Report ID: AC1040
Analyst Date
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2.005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
JRN 03/01/2005
Time
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
Davis & Floyd, Inc. I PO Drawer 428 j Grei:nwood, SC 29(148 I 816 E. Durst Avenue I Greenwood, SC 2%49 I (864) 229-4413 j Fax (864) 229-71·19
DAYIS
FLbYD
Client
Contact
LABORATORY ANALYSIS REPORT
TICONA, LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Certification Number: 25
Project Number: 61621.01
Report Date April 18, 2005
Page 74 of 88 Report ID: AC1040
QC Batch Report -Method Blanks
WorkGroup: WGt0388 Matrix: GW/ChemW
Bl:ank MB403881l
Prep Procedure Method Analyst Prep Date
Analytical Prep Proceduresz
DOWTHERM SW846 35008 DBC 02/22/2005 0800
8270 svoc PREP SW846 3510C DBC 02/22/2005 0800
Davis~~ Floyd, lnc. ) 1-'0 Drawer 42H I Creenwond, SC 29(l48 I 81 (, I:. Durst Avenue I Greenwood, SC 29(,49 I (864) 22:J-44I J I fax (8(i4) 2n-7 I 1 '.J
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DAYIS
FLMD LABORATORY ANALYSIS REPORT
1,1'-BIPHENYL
BIPHENYL ETHER
1,1'-BIPHENYL
BIPHENYL ETHER
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem carter
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 75 of 88
April 18, 2005
Report ID: AC1040
QC Batch Report -Matrix Spikes and Duplicates
WorkGroup: WG40388
MS/MSD MS05022007-02:40388
MSD05022007-02:40388
o.osoo
0.0500
0.0500
0.0500
Matrix
Prep Method
GW/ChemW
SW846 35008
Analtyical Method: SW846 8270C DOWTHERM
Not Evaluated See Note Below.
Not Evaluated See Note Below.
Not Evaluated See Note Below.
Not Evaluated See Note Below.
NOTE: MS/MSD t recoveries are not evaluated if the sample concentration is greater than four times the spike added.
Davis & Floyd, Inc. I PO Drawer 428 I Creenwnod, SC 2964B I 816 E. Durst Avenue I Creenwood, SC 29fi49 I (864) 229-4413 I Fax (864) 229-71 !9
DAYIS
FLMD LABORATORY ANALYSIS REPORT
1,1'-BIPHENYL
BIPHENYL ETHER
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Fem Carter
NC Cenification Number: 25
Project Number: 61621.01
Report Date April 18, 2005
Page 76 of 88 Report ID: AC1040
QC Batch Report -Laboratory Control Standards and Duplicates
WorkGroup: WG40388
LCS LCS403881l
0.0500
0.0500
0.0398
0.0388
Matrix
Prep Method
GW/Chemw
SW846 35008
Analtyical Method: 8WB46 8270C OOWTHERM
mg/1
mg/1
80
78
40-108
42-109
Davis & Floyrl, Inc. I PO Druwer 428 I Creenwood, SC 29b48 I 81 (i E. Durst Avenue I Creenwood, SC 2%4~J I (8(14) 22'.l-441 J I Fa;,,: iH64) 229-71 19
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DAVIS Fibito LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem carter
NC Cenijication Number: 25
Project Number, 61621.01
Report Date April 18, 2005
Page 77 of BB Report ID: AC1040
QC Batch Report -Batch Sample List
WorkGroup WG40471 Matrix GW/ChemW
□e._scription: SV/8270/BNA/TCL SV/DOW Prep Method SW846 3500B
Analtyical Method: SW846 8270C DOWTHERM
PREP ANALYTICAL
Sample ID Client ID Run# Date Time Date Time Analyst
LOS022303-01 PEW-1 1 02/28/2005 0800 03/03/2005 1238 JRN
L05022303-02 PEW-3 02/28/2005 0800 03/03/2005 1438 JRN
L05022_303-02 PEW-3 2 02/28/2005 0800 03/03/2005 1756 JRN
L050223 03-03 PEW-4 1 02/28/2005 0800 03/03/2005 1557 JRN
L05022303-04 DUP-4 1 02/28/2005 0800 03/03/2005 1636 JRN
L05022812-01 FB-01 1 02/28/2005 0800 03/03/2005 1715 JRN
MB40471:l Method Blank 1 02/28/2005 0800 03/03/2005 1005 JRN
LCS40471:l Laboratory Control Spike 1 02/28/2005 0800 03/03/2005 1530 JRN
MS05022303-01:40471 Matrix Spike 1 02/28/2005 0800 03/03/2005 1319 JRN
MSD05022303-01:40471 Matrix Spike Duplicate 1 02/28/2005 0800 03/03/2005 1359 JRN
Dilution
1
4
10
1
1
1
1
1
Davis & Fluyd, !nc. I PO Drawer 42B I Greenwood, SC 2%48 I fl 16 E. Our~t Avenue I Greenwood, SC 2~h-l9 I (864) 229-4413 I F;.ix (864) 229-71 19
DAYIS
FLtrYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Cenijication Number: 25
Project Number: 61621.01
Report Date
Page 78 of as
April 18, 2005
Report ID: AC1040
QC Batch Report -Surrogates % Recovery
WorkGroup: WG40i71
L05022303-01 03/03/2005
L05022303-02 03/03/2005
L05022,303-03 03/03/2005
L05022303-04 03/03/2005
L05022812-01 03/03/2005
MB40471:l 03/03/2005
LCS40471:l 03/03/2005
MSOS022303-0l:40471 03/03/2005
MSD05022303-0l:40471 03/03/2005
FBP -2-FLUOROBIPHENYL
1238 43
1438 93
1557 60
1636 79
1715 64
1005 78
1530 78
1319 80
1359 83
Matrix
Prep Method
GW/ChemW
SW846 35008
Analtyical Method: SW846 8270C DOWTHERM
Davis & Floyd, Inc. I PO Dr;-iwer· 4:!U I Grecnwr.iud, SC 2%48 I 81 () E. Durst Ave;nuL' I Grec11w1Jod, SC 1')h49 I (864) 229-441 :\ I Fax (Hf.4) 229-7119
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DA~IS
FLMD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
QC Batch Report -Method Blanks
WorkGroup: WGt0•71
Blpnk MB404711l
Parameter
Semivolatile Organics
SW846 8270C DOWTHERM
1, l' -BI PHENYL
2,3-DIHYDROXYBIPHENYL
BIPHENYL ETHER
Prep Procedure
Analytical Prep Procedures:
Method
'
'
'
DOWTHERM SW846 3500B
Result Qual
0 .010
0 .025
0 .010
Analyst
DBC
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 79 of 88
Matrix: GW/ChemW
RDL Units
0.010 mg/1
0. 025 mg/1
0. 010 mg/1
Prep Date
02/28/2005 0800
April 18, 2005
Report ID: AC1040
Analyst
JRN
JRN
JRN
Date Time
03/03/2005 1005
03/03/2005 1005
03/03/2005 1005
Davis & Floyd, Inc I PO Drawer 42S I Greenwood, SC 29648 I 816 E. Dur.sr Avenue I Creenwo<>d, SC 29649 I (Hf>4) 229-4413 I Fax (864) 229-7 ! 19
DAVIS
FLij-YD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Cenijication Number: 25
Project Number: 61621.01
Report Date
Page BO of 88
April 18, 2005
Report ID: AC1040
QC Batch Report -Matrix Spikes and Duplicates
WorkGroup: WG40471
M~/MSD MS05022303-0l:40471
1,1'-BIPHENYL
2,3-DIHYDROXYBIPHENYL
BIPHENYL ETHER
1,1'-BIPHENYL
2,3-DIHYDROXYBIPHENYL
8 I PHENYL ETHER
NOTS: MS/MSD l recoveries
MSD05022303-01140471
are not evaluated
0.0500
0.100
0.0500
0.0500
0 .100
0.0500
if the
Matrix
Prep Method
GW/ChemW
SW846 35008
Analtyical Method: SW846 8270C DOWTHERM
< 0.0100
< 0 0250
< 0 0100
0. 04 03
0.0250
0 0388
0.0382
0.0250
0.0364
mg/1
mg/1
mg/1
sample concentration is
mg/1
mg/1
mg/1
81
0
78
greater than
76
0
73
5
0
6
four times
34-102
18-125
31-110
JO
15
31
34-102
18-125
31-110
the spike added.
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 ) 8 ! 6 E. Durst Avenue / Greenwood, SC 29649 I (86-t) 229-4413 I F;1x {864) 229-7119
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LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Certification Number: 25
Project Number: 61621.01
Report Date April 18, 2005
Page Bl of 88 Report ID: AC1040
QC Batch Report -Laboratory Control Standards and Duplicates
WorkGroup: WG40471
L~S LCS404711l
1,1'-BIPHENYL
2,3-DIHYDROXYBIPHENYL
BI PHENYL ETHER
o.osoo
0.100
0.0500
0.0376
0. 0711
0.0360
Matrix GW/ChemW
Prep Method SW846 3500B
Analtyical Method: SW846 8270C DOWTHERM
mg/1
mg/1
mg/1
75
71
72
40-108
39-103
42-109
Davis & Floyd, Inc. j PO Drawer 42.rJ I Creenwood, SC 29648 I 816 F.. Durst Avenue I Crcenwood, SC 2%4:J I (8(i4) 229-•l4 I 3 I Fax (a64) 229-71 ! 9
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Cenijication Number: 25
Project Number: 61621.01
Report Date April 18, 2005
Page 82 of 98 Report ID: AC1040
QC Batch Report -Batch Sample List
WorkGroup WG40535 Matrix GW/ChemW
De,scription: TOC GW Prep Method
Analtyical Method: SW846 9060
ANALYTICAL
Sample ID Client ro Run#
PRBP
Date Time Date ·Time Analyst Dilution
L05022401-0l V-23
L05022401-02 K-28
MB4053?:: 1 Method Blank
MB40535:2 Method Blank
LCS40535:l Laboratory Control Spike
LCS4053S:2 Laboratory Control Spike
MS05022402-02 40535 Matrix Spike
MS05022407-05:40535 Matrix Spike
MS005022402-02:40535 Matrix Spike Duplicate
MSD05022407-05:40535 Matrix Spike Duplicate
03/03/2005 2002
1 03/03/2005 2027
1 03/03/2005 2327
1 03/04/2005 0435
1 03/03/2005 2255
1 03/04/2005 0404
1 03/03/2005 2205
1 03/04/2005 0311
1 03/03/2005 2223
1 03/04/2005 0328
CDC
CDC
CDC
CDC
CDC
CDC
CDC
CDC
CDC
CDC
1000
25
1
1
1
1
Davis & Floyd, lnc. I PO Dr;iwer 4211 I Creenwnod, SC 2%48 I 816 E. Durst /\venue I Greenwood, SC 29649 I (B64) 22';.l-441 J I Fax (864) 229-711 1)
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D_AYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 29152
Pem Carter
QC Batch Report -Method Blanks
Parameter
Wet Chemistry
SW846 9060
WorkGroup: WG40535
B\ank MB405351l
ORGANIC CARBON, TOTAL
Result Qual
< a.so
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 83 of 88
Matrix: GW/ChemW
RDL units
April 18, 2005
Report ID: AC1040
Analyst Date Time
0.50 CDC 03/03/2005 2327
Davis & Floyd, Inc. I PO Dr,1wer 42B I Creenwood, SC 29648 I 816 E. Durst Avcttue I Greenwnocl, SC 29649 I (864) 219-4413 I Fax (864) 229~7 I 'I 'J
DAYIS
FLMD LABORATORY ANALYSIS REPORT
Client
Contact•
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
QC Batch Report -Method Blanks
Parameter
Wet Chemistry
SW846 9060
WorkGroup: WG40535
B~ank MB40535:2
ORGANIC CARBON, TOTAL
Result Qual
< 0.50
NC Cenijication Number: 25
Project Number: 61621.01
Report Date
Page 84 of 88
Matrix: GW/Chemw
RDL Units
April 18, 2005
Report ID: AC1040
Analyst Date Time
0.50 mg/1 CDC 03/04/2005 0435
Dew is & Floyd, Inc. I PO fk1wer 42H I Greenwond, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-44 l 3 I Fax (864) 229-7119
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DAllS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Cenification Number: 25
Project Number: 61621.01
Report Date April 18, 2005
Page 85 of 88 Report ID: AC1040
QC Batch Report -Matrix Spikes and Duplicates
WorkGroup: WG40535 Matrix GW/Chemw
MS{MSD MS05022402-02:40535 Prep Method
MSD05022402-02:40535 Analtyical Method: SW846 9060
ORGANIC CARBON, TOTAL 10.00 6.69 17.00 mg/1 103 74-125
ORGANIC CARBON, TOTAL 10.00 16.50 98 3 11 74-125 I NOTB: MS/MSD % recoveries are not evaluated if the sample concentration is greater than four times the spike added.
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I D,1vic-,~ Floyrl, Irie. I r'O Drawer 42B I Gt"(::enwood, SC 2~164B I 816 E. Durst Avenue I Greenwood, SC 2':)b49 I (864) 229-441 J I F<tx (864) 229-7119
DAYIS
FL(JYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 86 of 88
April 18, 2005
Report ID: AC1040
QC Batch Report -Matrix Spikes and Duplicates
WorkGroup: WG40535 Matrix GW/ChemW
MS{MSD MS05022407-05140535 Prep Method
MSD05022407-05:40535 Analtyical Method: SW846 9060
ORGAN"IC CARBON, TOTAL 10.00 1. 66 12.20 105 74-125
ORGANIC CARBON, TOTAL 10.00 11. 80 mg/1 101 3 11 74-125
NOTB: MS/MSD \ recoveries are not evaluated if the sample concentration is greater than four times the spike added.
Dc1vis & Floyd, Inc. I PO Dr,1wer 42/l I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-4413 I Fax (864) 229-71 ·1 9
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DAYIS
FLtfYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA, LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Certification Number: 25
Project Number: 61621.01
Report Date April 18, 2005
Page 87 of 88 Report ID: AC1040
QC Balch Report -Laboratory Control Standards and Duplicates
workGroup: WG40535 Matrix GW/ChemW
LCf LCS40535:l Prep Method
Analtyical Method: SW846 9060
ORGANIC CARBON, TOTAL 25.00 9.92 mg/1 99 90-110
O;,vis &.· Floyd, Inc. I PO Drawer 428 \ Creenwood, SC 29648 I 816 E. Durst Awnue I Gret.'nwoorl, SC 29649 I (B64) 22<J-4413 I F,ix (864) 229-71 I 9
Df\YIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Pem Carter
NC Cenification Number: 25
Project Number: 61621.01
Report Date April 1B, 2005
Page 88 of 88 Report ID: AC1040
QC Batch Report -Laboratory Control Standards and Duplicates
WorkGroup: WG40535 Matrix GW/ChemW
LCf LCS4053512 Prep Method
Analtyical Method: SW846 9060
ORGANIC CARBON, TOTAL 25.00 9.96 mg/1 100 90-110
D:wis & Floyd, Inc. I f'O Drawer 4.'.rn I Cree11woocl, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29()49 I (Rfi4) 229-4--113 I F:i.x (864) 22~)-7! 1 Y
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D\YIS
FLOYD LABORATORY ANALYSIS REPORT
Method Conformance Summary
Client: Ticona, LLC Project Number: 61621.01
Login(s): L0502 l 803, L0502 l 805, L050022007, L0502303, L05022401, L05022812 Report Date: April 18, 2005
Criteria Volatiles
Sample Holding Time ✓
Standards Preparation ✓
Instrument Tuning ✓
Instrument Calibration ✓
Calibration Verification ✓
Degradation Check NIA
Interference NIA Sample/Standard
Blanks Results ✓
Method Accuracy •
Method Precision ✓
Surrogate Recovery ✓
PDS/SD/MSA NIA
TCLP Preparation NIA
✓
NIA
Method Criteria Met
Not Applicable
1,4-Semi
Dioxane Volatiles
✓ ✓
✓ ✓
✓ ✓
✓ ✓
✓ ✓
NIA NIA
NIA NIA
✓ ✓
✓ •
✓-•
✓ •
NIA NIA
NIA NIA
* Method Criteria Not Met -See footnote(.,) below.
PDS =
SD =
MSA=
Post Digestion Spike ·
Serial Dilution
Method of Standard Additions
TOC
✓
✓
NIA
✓
✓
NIA
NIA
✓
✓
✓
NA
NIA
NIA
Footnotes: Volatiles-1,2-Dichloropropane on WG40376 exceeded the established lower limit
of91 % (85 and 90) for the MS and MSD respectively). The LCS associated with
this batch recovered within acceptable limits.
Semivolatiles -Includes Dowtherm.
Semivolatiles-Surrogates on WG40388 exceeded the established limit for FBP, 2FP
and PHL. Multiple matrix spike failures were present in the MS and MSD. All
failures are associated with sample L05022007-02 indicating a sample matrix
interference. Surrogate recoveries for the method blank and LCS were within
established limits.
I Davis,, Floyd. Inc. I F'O Drawer 428 I Creenwood, SC 29648 I 816 E. Durst ,\venue I Creenwr.,nd, SC 296-19 I (864) 229-4413 I Fax (8641 229-71 I 9
~
~y Chain of Custody Record
ClientJ::-.'tJ$1t. / .,,,,.,, _ J, _,, . . -1vl;L f,:1ffuC:1A-'i?S-
Address r;:;_ ,0 <.3a)( §r:fJ.i/7
CUy 5'. (j) /A-< J!fcVVttiC I State 1 Zip Co<je JL ~txfc,•
Project Name C;v4-/T7[,ru(J-
Project No. ,
P.O. No. .2 &-.? t(}.J ;s----
Sample ID I Description Date
(Containers for each sample may be combined on one line.)
SHEALY ENVIRONMENTAL SERVICES, INC.
136 Vantage Point Drive
Cayce, South Carolina 29033
Telephone No. (803) 791-9700 Fax No. (803) 791-9111
Report to Contact Te'::Jlp}ne No. I Fax No. I E-mail , /J'4f/ -:J2--;2 fl, ,t.J3,p__ •. '&,y/-'/ t-2 _yt('lll ,J · 9f.2. ,r .J<-19
Waybill No. I
Quote No.
Page l D/
Sampie,'s S:J:?tu,e ' L ~ ·--,.
,. Analysis (Attach list if more space is needed.) l x./ '"7/_ .
Printed' ..
t:.--nt:trc!J2 1 ';. /:-iNJ,'t,,+,,,_ _; ~~ No. of Containers Lot No.
r§ 1 Matrix by Preserv<:-tive Type
t,? ~ i " ~ . nme ~o ~ ... 5 s ~ 8 1, ~ .,. il •• § ~ ~ ~ 8 ~ ~ :z: ~ ~ ~ Remarks I Cooler /.0. ' a
L
l
V-13 Z/23/,;i-09f-< ~ X 3 I X X _t;-~'7¾:k-cP-f).,,7-_
)::-Jf ¾ii,; )71-< t-X 1 I ·-,f2rfl /Jtkufi -I 'l/4,{1,..-09a, / X 2 J
,,.,...---·) /)
Sample Disposal
)(
X
K 1r :Jt;t;sS--
li:-Pr-p.reu-·t'zyt: ttJm\ ,fr
IJc /, N.\.2., S z_{; 5
'ffie-,1s""c 2.1l1Lc' I < -.~c_
/4.-~t,tl,--;T 0,:.1 2.:::.v,4
f:tqj1:.iJ2:'J /i' -'l s ,t,.,)
f 9
r-.is:)
Note: All samples are retained for six weeks from receipt
POSSible Haz7□ntificati~Ij
□ Non-Haza □ Flamr,(able □ sLtant/~ Poison □ Unknown □ Retum to Client fDisposal by Lab unless other arrangements are made. Tu~ A':;:IJ1~fred (Prio_r iap/f required for expedited TAT.) ' QC Requirements (Specify) !.NeL "X 1uStan ush(~
( 1. ~ . edby .',h c,(' --D~/2.✓.i-Time _ 1.Raceivedb~ ,.L J / J :J.-2]()_') Time / ~· r't2..J l{;,2S ,,,,,,,...,. .,._., / -It; 2 \ ,--"'fc/ -,:/ fl_A,,,A I 2.~-7~ ltlate ;;2-23-0S T7~_s 2. Received by Date Time
3. Relinquished by Date Time 3. Labr;'';;","s~by hL-" (/1 j I Data Time
,( 1.r{tJ ,:;-17~s-Commenrs LAB USE ONLY ,J Received on ice (Circ/e{;;;)No Ice Pack Receipt Temp. "C --
-
---
~-- -- -------SHEALY ENVIRONMENTAL SERVICES, INC. sey Chain of Custody Record 106 Vantage Point Drive
Cayce, South Carolina 29033
Telephone No. (803) 791-9700 Fax No. (803) 791-9111
,
Client r-,_,. ~ /' 7!2 /t( Report ~ntact J:l-611.. /J
Te/epf]one ~Fax '3'fj:-mail ~ ~ . Quote No. ',, -ft/ . {, Jd"t /,fJeT '--6fUZ) .../tPf·-· _7.9 'fo / ;t;-'/:2 ,r.?£~ ~ ,
Address,H) }!, tJ ;( <fi1Jt;7 Sampler's/ignat~~. ~ _ Waybill No. / Pa:J.;_f,_ of j_
Cily {, (J ,~r l~ul> ~/, /l-, Analysis (Attach list if more space is needed.) -I _ 11'1 '([/;Jf/1,t.[-,.
Project Name C~4 /T;'tu-vA--t)t&,4"] 'T. /tft,41,liJL, V, Project No. J6&-:.S1J PO. No. ~ No. of Containers ),/i'f$;:-_& Lot No.
o• Matrix by Presen.;ative Type ~ ,'(~~ ·.\: G~ t Sample ID I Description Date Time "0 ~ ~ ~ ; I~ i5 ~ -;!_ '7 ~ ~" 1 ~ ~1 (Containers for each sample may be combined on one line.) ~ ~ ~ ! ~ ~ ~ ~ Remarks I Cooler ID. ' ' •'P_,,Sk l(f,;/,. tflo / X ? I')( -~e-r 7;4¢.c!il~ ..,
f-,_s:-5" I .c,~· l ( X x )< 1f")'t.4JJiJ ,tr, ~i~ \)) -6
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."&tf ,.~ 'r 6~ ./ ;!.;>;' -, IJ/t1.Ni_1S20, As -
f/l(J!'EPZ11..i-:Pv£
Possible Hazard Identification // Sample Disposal Note: All samples are retained for six weeks from receipt
□ Non-Hazard □Flammable □ Skin Irritant/ Q.Poison □ Unknown □ Return to Client 1 i'bisposal by Lab unless other arrangements are made.
Tum Around Time FJeqi/ired (Prior lab approvar'roqµ,red for expedited TAT.) QC Requirem__~nts (Specify) LCVP-:~ •? ; •• ; I 11a'Strmdard /{l/"8ush /Spedty) / / /
/ t. RelinquilitJed by ::[" 'j,-/ ~-·· l~~r-T7r.r-; I. r:,-ceJf~/)'/rd_,/ _,:~,.,, Date Time .f4 , , /
Z-/?o~/ .... / ;_{"7 .,,,,~· /,,,t~ ,_.,, .,,:; __ ,. 7~ ' -
2. Rslinq~ish.ecf. by\,, ,;(,, 1 -✓-.,/ _. Date Time -;)( 2. Received by Date Time / -f:::.-"cfl./J( '/J/:.._ _,(,,/~ -;:;::, "?-/ f!',. 0 '5"" /,f's-' , .
/ 3. Relinquished by Date Time T/s';r/ rec("" b/Jl. G, ( /J ,, Date ;!},me/ /J. 5 7 J. -1,fLJ!-
Comments LAB USE ONLY
Received on ice (CirclB) Yes No Ice Pack Receipt Temp_ ·c
DISTRIBUTION: WHITE & YELLOW-Return to laboratory with Sample(s); PINK-F!s/d/C/Jent Copy
-
~ SHFALY
~ Chain of Custody Record
Client t: J/,A{ ---f</ fli. jp(; --(-;,,c_/~
Address <Po ~Y S:-o:147 .
City s 1,/4 ft. 6J,,J VI 1.-tE [;~ lz;~6fo
Project Na~A-J. 7CoNA-PtojectNo:Jli,~s I~ PO. No.
Sample ID I Description Date
(Containers for each sample may be combined on one line.) .
'1>0P-/ l
2}li£
S-J
-1 ..J_ (
SHEALY ENVIRON!I/IENT~L SERVICES, INC.
106 Vantage Point Drive
L U 0 0 :A If? 0 3
Number 43003 Cayce, South Carolina 29033
Telephone No. (803) 791-9700 Fax No. (803) 791-9111
Report to C~nt~t ,. ~ ,;., ~ "'1l:: "'1!4'-'7 .. Te~No. rgx No. I E-m/J Quote No.
f✓ < , -. . ·. ~,..Z,tL· -9 ',,) 9¥9.,1, ~-9~-...a.,
sazu,e ,£-Waybill No. I
Page Pot __
X . p •· Analysis (Attac~ more space is needed.)
Printed~ / ..
"~ ~~. 7: 14-£/4.,fv /4~(# ~, No. of Containers #, Lot No. Matrix by PreseNative Type UE I ~~ ~ /J~j nme "° ~ i ~ ~ Ii uu I ~ -~ ~ , ~ ~ Remarks I Cooler 1.0. < < ,
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' Possible Hazard Identification □ Ski/4nl□ Poison
Sample Disposal Note: All samples are retained for six weeks from receipt □ Non-Hazard zf}:lammable □ Unknown □ Return to Client I' Disposal by Lab . unless other arrangements are made. ·;r Ay~~uired (Prior o/pp7 required for expedited TAT.) f QC Requirements (Specify) Lev a :.zr:. Stan Rush (Specify) ;
I~ {,Ashed by 7/j// -l;tl,1.lr o/?)d 7Rec?J:o/ ;0~ ff °!.JI 7 /4.._ Time / 7 -7.' U -' -2.Retinq#~//V/4 ,'/'--l~f¼ 7, 05 1/9.35 2. Received~ Date v Time
3. RelinQllished by Date 1 Time rlls£ sed 'fx_,c; (;,(I._,, 1 ~ate/JO<: l.Iime !~ 1..<J . I. . . Comments LAB USE ONLY
Received on ice (Circle) Yes No Ice Pack Receipt Temp. "C TRIB - -
WHt-LLO._,tol..., with-(s); P-<VCt; .... --
-
------
-- --Chain of Custody Record
C/Jent t· ,/? A Ub l-f;_,?/f t,fSl,rt:/,f'lkf
Address n, 7sc1x /0,;ll/7 c;'r,, . -!Al PftJNil/£;{(" ~r· I ;t;2J-a
Project Name I
C.AJ,4-/ I /C-oV.4
Project No. ,;2 [, 4f'J~ PO. No.
Sample ID I Description Date
(Containers for each sample may be combined on one line.) I
------------SHEALY ENVIRONMENTAL SERVICES, INC. L o 5 0-~ / 9 O 5
106 Vantage Point Drive N 4 •') Q Q 1
Cayce, South Carolina 29033 um er · ,.) .
Telephone No. (803) 791-9700 Fax No. (803) 791-9111
Report to Contact --r-Li .---.,-,,--, 6~ Tefe~e No. I Eax.No. I ~I /~ .. Quote No.
flr..,,J...,/;:Jl.K . , .. '&'-(-y/;,J-9 r1/w/-f!t,') ~;1/ / ---y saztu,e ~ff· Waybill No. Page_L ofd_
X ✓,~/~~ ·· Analysis (Attach list if more space is needed.)
Printe~~ -'
,.
j7Z,p.,tl'/Z'7 I< ~,l)JflVf'l_)
• No. of Containers v, Lot No. ~T Matrix by Preservative Type ~· "
\'j
Time il;?, ~ ~ 2 ~ g 8 -~ 5 :ii § ~ J a 1., ~ ~ ~ f a Remarks I Cooler f.D. < < ~ ~
Jl}/-7·7 r¾·it /,J~ t '· I' ' ~z . /,l}ffc~;zi).:
-
!Ill-L/R /3,(f ~ o?tt1?-.(
. ' J,S
C-'/C/ /~v r;:--3'/ lb/1 :f.. Uv v,.nJ ?.it:<ft/ll,'lil fr-b). 4 I 7cr-; • /ft.,f,t,,,,,N,_9S1.tJ1 t~1,
--rJ:-,p 'JJL4/lJK -~ :l 1, ·/ -J</:fb ~~
t';;--t, I ~I,,./ / /j /{130, '?
1-3-r-' ! 1:J'-!t)
14A-s1 /433
£1:---5-,f ' Jl(3 '
,,, . ' Possible Hazard Identification // Sample Disposal Note: All samples are retained for six weeks from receipt
□ Non-Hazard □ f;i£1mmable □ Skin lrritctnf ..tJ Poison □Unknown □ Return to Client . / Disposal by Lab 1.mless other arrangements are made.
~ Arou~Zi Required (Prior lab approiia'ruired tor expedited TAT.) , QC Requirements (Specify) iEVn-rr:. pf/ / / Standa /. _ 0'Rush (Specify) _ / / •
,-1, Relin<lfShed by ' I --~ -0~11-/4 T'7'7)D 1 Received"[/ J :-:/ i/ / i:f 1/i '/;: Time
/" f,tf?-77 -_, /" ... .,. ,r:( 1 as l7~C "2. Relin/r/'/// #, ~ ~ ' 13/, ',Ji 11'"iq35 2. Received by , Dare I Time 17 <
3. Relim;Jl,1ishecJ by ' Date Time
~ra,o,y ·~ ln c-r: u Date rl'772.D 'I"> A_,, J • •~ ., _17.(),5
Comments LAB ()SE ONLY
Received on ice (Circle) Yes No Ice Pack nece1pl Temp. "C
DISTRIBUTION: WHITE & YELLOW-Retum to fa_boratory with Sample(sJ: PINK-F1eld/Chent Copy
~
~y Chain of Custody Record
Clientt,.· ,_... ,_,'l,;Jt -,n., ?,t f,f.C{'tJc1.,r7e--.r
Address 0 feJj-<fc:,:J $1 )
CUyJ,. I,{,,'? ./4-,,.,f/1-l ,c:-~~· I ".2?uo
Project Name.---;-
I/ Cct/1/ /J
Project No. ;?t,r0.r1.r PO. No.
Sample ID I Description Date
(Containers for each sample may be combined on one line.)
?e-u-I 2/41 l7, -,:,'
7EZu-3
(y£LJ-i
SHEALY ENVIRONMENTA!.. SERVICES, INC.
106 Vantage Point Drive
L U!J U li. ~3 03 .
Number 43011 Cayce, South Carolina 29033
Telephone No. (803) 791-9700 Fax No. (803) 791-9111
Report to Contact •. Tefe~h_one N9. _I Fax No. l_,,E-ma¼, <> _ . Quote No. ✓€?</lY ,E.,,,z,b J&/. J7?9. -:?'fro /1~·/t,? ~;3:,9 ~2natu,~? Waybill No. /
PageL o, L
PrinWdN~
•Analysis (Attach list if more space is needed.) ,.
C~ai., 'T. ,k I ,vf,t( 1>-r..J ~11~ -~ No. of Containers Lot No.
~f Matrix by Preserv_ative Type ~. ~ ·I ~ y ~~ Time ~8 ~ ! g 8 :-[f 6 ~ ! ~, ~
< •• ~ i' ' ~ ~ Remarks I Cooler I.D.
/3£/3 V ,,. X )( X Sa:-") ,,fi-k afl.~c><.
i</-0 X l-' X ..,P::_;16,f'JXJ
t1t(3 X X K
'ou'?·-'-1 t --p )( ic )<
'TP-t fl Pltfllk. -3 ·2-/2,r o9oo ~le I~ IX
:f. ?l6c~t/,ffll £( lw'Jl.
A, ;/ct 4,2..J~.tl -r.
Possible Hazard Identification □ Skin ,,L, /2 Poison
Sample Disposal Note: All samples are retained for six weeks from receipt
□ Non•Hazard ~mmable □ Unknown □ Return to Client ~"Disposal by Lab unless other arrangements are made.
Tum Aroun~'equired (Prior lab 7,v,Y,}egtJired for expedited TAI) OC Requirements (Specify)
.L,6V~-Z.... 'JI-f.J}. Sta.nd,,j;J, Rush (Specify) ;1 /
/,,iliishedby Ji~ < OaX,,/4 17:1~ 1. Received½ ... ~h / Date Time 1...--; ..... ,'. z,, 'k ·IS-,.,.. /'hl-,1,-~ ?·;?,?d6 /__y.'? L ,;::~, "'--2.Re/i~ ror.L/J:A-i ' , ,
Date Time 1uate Time 2. Received by #-f,/,5 /'?tPS
3. Refi~uished by Date Time 3. Laboratory receiveh? /} Date Time JJoS--T1.s11 S' L, C, C,M If. J, !{,_ oS
Commems LAB USE ONLY
Received on ice (Circle) Yes No Ice Pack Receipt Temp. "C
... IBUW.,,HIT,...LOW-tola~th,_,);P/,...Clie--- --- ----
I
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Purged Well Sampling Log
Project No. Kubal-Furr & Associates
-E,rviro11111c11t11l Co11s11/tn11l1-Sile Location CNA Holdings/Ticona, Shelby, NC
Field Personnel G-1!.. I '3 5
Well/ Sample ID
Weather Condition v:v4l SwM,
Semple Dale 2 / f s-/ c,~ Arrivol Time II 2Lf Sample Time_--t-.-'-'~-+----
Descriplion of Measuringl,...,.,r 6l,,' I c . 1 @J.s L k' c [2J Casing~ Po·,nt (l,'P) i" os1ng ype oc. 1ng op V 0. 1 1 v
1ome er ir.ch"?s
Total Depth of Well Below! L/ L/. ~ Q I
t,,IP?_ l~•~t Common Gallons oer Foot Conversions
::=====:::::::
Depth lo Waler Below ~IP?I 3 ')5, 95' ,.J
::=====::::::::::
Colur:,n of \Noter in Well'?( i O : q 5-k·ell ::===::::::::=::::::::::
Gallons oi Wol~r per f..,o:I {J, IG3
a 0,110°"
[see chart)?
Go!/ons of Water in Well? L ,g cell
Gallons of Waler to be 5, 3if. J Purged i3X)?
Purge Method? 6 Cli{(/ I
Purge Storr Tin;e/ t 3i i I
Initial
1 1/4 in Well Casing= 0.064 gal/ foot
1 1/z in \Nell Cosing = 0.092 gal/ loot
2 in Well Cosing= 0.!63 gal/ foot
3 in We/I Cosing= G.367 gal/ toot
3 1/:_ in Well Casing= 0.500 gal/ fool
4 in If/ell Cosing= 0.653 gal/ foo:
6 in Well Cosing= 1.469 gal/ foot
Total G0l!ons Purged/ 1) goll
Purge Stop Time( I 33·2 I . 2 3 4 5
Samples Collected Container De5crip!ion Preservative
@-1,v>-,___ c~ y-1:rL2i
i'l:,~4
!G.42-
Remarks ________________________________
_
Parameler Conditions: pH
Turbidity
+/·0.1 standard unit
+/-!0% above 10 NTU
COND/Temp +/. 3%
+/· I NTU below 10 NIU
DO
ORP
+/-1 G%
+/-!OmV. ..
Revise 5/28/02
Kub JI-Furr & Associ.1tes
P,x:;-o: 1:-,·:--.,:c': {-ie (x"'~fl'.j
;,,~r.;,= ~~-:::-: 7·,-.1~: // :S: 1;2.
·,,:cter-Level 1\\eoiuremenf5
: .. ~
11
" (,I.)
iJ
: 5
"
17
13
"
20 I
I
S-:;rr-ples Coile<;; ttld t/4%,
9
IO
II
"
13
"
15
16
17
,a
19
20
---
7
7,
I 7,
Field Poromer:;;rs
c--~. -·~--..:.
i.·~~-·c:-::i t.',TL'I
[:,;;:;· • .,i,:
0,·,-;::a,-.
(mg1~J ·-
Cor.t::iiner De;c1:::.:::::.,
g '< tf.0.i t It~~. " z:s'lh. ------.u~ . .,.,,, -;, ) .· .· 7"
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Pcoject t:o. _ __,,J_(c,_, 6__,,_e_jl_--J_ Kub.11-Furr & Assod,ltcs
-£1;:·in>11nt,·n.'<1! (p11_,1d.',111/;;-
5
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field Porcime:e-rs
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lo·.v-f!01•.G:ovodwci!er s~"';:i:;:1g L::ig
Kub,11-Furr & .--\ssocijtes
-£1:;•i,-,,11'1:c•:1:,:: Cc>ll,C/l/;,111.'_; -
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Vioter-Levei ,'.teasurements
-~-,.ec·•.~ -----· • D;-.,., (:ee:; l" .,
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" ! 70 I ;1.,fo I'
15 ' '7s I ! 1-t,;J/ IS
16 ! I IS
17 ! ! 17
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19 I I 19
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Lo·...,.fjzy,~G,o·;:,d.--o'd' i::-rc·i,,c Log
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Low-Flov,· Grcundwo;er Sampling Log
Kub,1l-Furr & Associates Pro_iect No.
-Ei:,·it("1111i•11tnl Cu11:-1dt,111t::'-Site L:Jcot,'on _C=Nc:A,_./Te,iC:.,Oe_nc,ac:•..:S:,.:hece,olb'.Ly,_, ,_,N_,,Cc......
Field F'erscnne/ _G=,-'.;..(L~· 1-/"'/,'-"'-::,'~-----
Well I Semple 10 -'--r=.,_F_'_-~3c...i..L/ _____ _
Scmf.":i':! Jere 2 1· f )/(J S-r.:rscl Time I. <::,1;.5lher Condition _",2. 'J<vcr:Y>cc'-::::-+----"Lc,' ~c.l'.::'·:...'...:':.sC>c...'->::.' _
-l L--.J. Semple :"irr.e f Z.. -,.
:;e;,::•;c;1cn of ~,ieo!uri.~.g: f ((){___ i Cosin T• e! S lxl:ing Ccp!i l-/ i Ccsir; 2 I
?01nt IM?)i : g IP l S', 1 Dicrr.e;,:, r.:M"
Pi.;rge Met~cci e~~-,·skl h 0 Sampling Melriod!'=('e_==i/=~=:1:=<-=--.r=~c-."-'-,-·----"'""
?~rge St-:irt Time; I 5yr-I Purge !·.::p iime! f (_, j '-\
1Nater-Level Measurements Field Parameters
0
I
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3
'
5
6
7
8
9
10
II
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13
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16
17
18
19
20
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Elc;::.,se T1r.,e
(m,ns)
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Samples Collected
Rerm::r~s , :J l v
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3
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6
7
8
9
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12
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--
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:)isscl·1e:: o~·,.ge"'
(rr.g/') .
--I -' 4. 'i'i: i I 2/ <;-
7,,i.,7-i / zz., 7
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pH +/-C. l st~ndord uni: CQ~:O/Temp +/-3f,
+/-I NTU below 10 N:U
DO -i-lOf.
rurbidily +.t-10%cbove 10tJ71J ORP -:-IC~n.V
..
CNA/T;cona
Low-flowGro"!ndwoter Samp6ng Cog
Kub.11-Furr & . .\ssodates
-£11:•irt>i:1,:~1:'.,;; (,,lli///:.:11.'~ -
:cccele Coe, ?_ I IC ( c\ s
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"v'/oter-Level /1.i\emurements
0
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Field ?ara.";".eters
0 i _ ____. ! i ---
1---
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15
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17 17
18
" 19
20 20
Cor,:c:.1er De,c11ptiol'I
Pcrame:er Cond::icn,:
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11
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Kubal-Furr & Associ.1te5
-E1::·i:·t1•1111,·1: .;i Con;:1!:.;:::., -
wo,-:;r-Leve: f',,\eoiurernents
C ! 0 :~1.t.ff
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Somp•-:?s Co,lected ltz:(
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Frcfecccro. ~~-l--iQ_JI_~_
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Field Pcrameicrs.
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Cor.to,ne: De,cnpt:cri
4,93, S,'J
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0,2 .• -, 217, 'I
er J.3 i ;l1'r. o
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lo·,•,.f:owGro~•-~~,.of,;,r Sor,-;;inQ Log
Kub,1!-Furr & Associ,1t~s
-£.•1;•iic•1: ":,••::,;! C1•l!::'/l/t,11:!~ -
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1S' 37,tff
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8
10
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13
15
16
17
18
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Container Descri;:'.,on
Fie.,J Parameters
-!---1-
i./9 I l,, )Ji .:37
I l,,JJ( I "31
! G :;z.9 i 13
! /;,, 3 ~ I . / 0
l,,331 9o
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Kub.ii-Furr & .-\ssoci.ite5
-En:·:•·,,,:11:,·n:,1:' L,,1:-:1:i.-.;,::f -CNA/Ticona · Shelby, NC
cc,·,~g·,
C:·ic:"'a'.7r.
?v:;;::: ·,:➔,:-:c, f ,:.> c"-; ..J:cJ J ( ,.-5.:;,":"::•i:",,;; ,•.:2··:.:: /:e,• &,•"SL, J; (.(,. ... 0 f
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Field ? .::r0me \ ers
I ------! ' --i -i
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'
DO +/-I:,'.,
O'=:? +/-10rn'.'
\
\
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Samolino Loo-Grab Water Samoles
Project No. 26QS 1 s --'-~---
Sam p I e Date --!-:)1/_:_'J-.e.}-1--/2-=-t:_.l __
'7Dv-r Sample ID
Site Location GI.~ I Ticona -Shelby. NC
Arrival Time
Duplicate No. _l)~v___,_?_-_{,.__
Sample Time ~[_'s_{~3 ___ _
(-/:_ Field Personnel -------
Weather Conditions .JL'Jv-c~; {:,cf Sampling Method
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Remarks
Container Description
_$,-\{(,:).Lt I Preservative J/ Cf /l.-~7 J.O·
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Container Description
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Revised 7 /30/02
Somolinc1 Log-Grob Water Som oles
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Sample Date _______ _
Sample ID Dupl'lcate No. ______ _
SampleTime _______ 1
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Arrival Time
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Sample Temp. (°C) -----Spec. Conductivity(pS/cm) pH _______ I '
ORP (mV) Turbidity (NTU) __c _______ ,DO(mg/L) ______ _
Method(s) I
-------~---1
Container Description Preservative
Remarks
Kubal-Furr & Associates
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Revised 7 /30/021
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Kub.ii-Furr & Assod.ites
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DATA ASSESSMENT SUMMARY CHECKLIST AND REPORT-LEVEL II
Client ID:
Project Number:
Project Description:
Ticona, Shelby, NC
26RP21
02/05
Sample Delivery Group (SDG) Description:
Prepared By: Robert DeGaetano
Date: 07/12/05
Two aqueous samples and a field duplicate were collected by Kubal-Furr & Associates and
submitted to Davis & Floyd of Greenwood, SC for total organic carbon analysis. The D&F login
numbers were L050504 l O and L05050602.
CONTENTS LEVEL COMMENTS
II
Sample Results ✓ Data are considered Class A
Chain(s) of Custody (COCs) ✓ Satisfactory
Master Tracking List ✓ Satisfactory
Method Conformance Summary ✓ Satisfactory
Batch Quality Control Report ✓ Satisfactory
Trip/Field/Equipment Blank Report ✓ Satisfactory
Field Notes/Logbook ✓ Not reviewed
Discussion:
Samples were analyzed within hold time requirements and results were consistent with historical
data.
Class A = quantitative Class B = qualitative Class C = unuseable
Kubal-Furr & Associates
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Df\YIS
FLfilD
June 15, 2005
RICHARD RAMIREZ
CELANESE
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Report ID : AC1629
Page 1 of 13
LABORATORY ANALYSIS REPORT
Login Number
Project Number
Description
:L05050410, L05050602
:61621.01
:TASK ORDER #26QS16 -TICONA SHELBY PLANT
Dear Richard Ramirez:
We are pleased to provide the enclosed analytical results for the samples received by
Davis & Floyd, Inc. on May 04, 2005 through May 06, 2005.
A formal Quality Assurance/Quality Control program is maintained by Davis & Floyd,
which is designed to meet or exceed the EPA, NELAC or other appropriate regulatory
requirements. All analytical analyses for this project met QA/QC criteria and the
results are within the 99 % confidence interval for each method unless otherwise
stated in the footnotes. This report is to be reproduced only in full.
Feel free to contact our Client Services Representative at (864) 229-4413 if further
explanation of the analysis is required. Unless other arrangements have been made,
samples will be disposed of or returned 14 days from the cfate of the report. We
appreciate the opportunity to provide services to your firm.
Sincerely,
DAV'?ZZ~C~.VT,,IJ---t'f--
ohn H. McCord, Jr.
Laboratory Manager
I Davis & Floyd, Inc. ) PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229•4413 I Fax (864) 229-7119
Di\YIS
FLfilD LABORATORY ANALYSIS REPORT
Sample ID
LOSOSOU0-01
Wot Chemistry
SW846 9060
L0S0S0U0-02
Wot Chemistry
SWB46 9060
L05050602-0l
Wot Chemistry
SW846 9060
Client
Contact
CB'LANBSB
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Richard Ramirez
Master Sample Tracking List
Client ID
DUP-2
V-23
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 2 of 13
Date Collected
05/04/2005 0000
June 15, 2005
Report ID: AC1629
Date Received
05/13/2005 0819
05/13/2005 0923
05/18/2005 1630
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst ,\venue I Greenwood, SC 29649 I (864) 229-44-U I Fax (flfi4) 229-7119 I
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Di\VIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
CELANESE
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Richard Ramirez
Client ID: K-28
Parameter
Wet Chemistry
SW846 9060
Matrix
ORGANIC CARBON, TOTAL
GW/Chemw
Result Qual
52.7
NC Certification Number: 25
Project Number: 61621.01
Report Date June 15, 2005
Page 3 of 13 Report ID: AC1629
Sample ID LOSOS0410-01
Date Collected: 05/04/2005 0952
Date Received 05/04/2005
RDL units Analyst Date Time
l.O mg/1 CDC 05/13/2005 0819
I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-4413 I Fax (864) 229-7119
DAYIS
FLiJYD LABORATORY ANALYSIS REPORT
Client
Contact
CELANESE
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Richard Ramirez
Client ID: DUP-2
Parameter
Wet Chemistry
SW846 9060
Matrix
ORGANIC CARBON, TOTAL
GW/ChemW
Result Qual
50.1
NC Cenijication Number: 25
Project Number: 61621.01
Report Date June 15, 2005
Page 4 of 13 Report ID: AC1629
Sample ID L05050410-02
Date Collected:
Date Received 05/04/2005
RDL Units Analyst Date Time
1.0 mg/1 CDC 05/13/2005 0923
Duvis & Floyd, Inc. I PO Dr;iwer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 ! (864) 229-4413 I Fax (864) 229-7119
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DAYIS
FLtfYD LABORATORY ANALYSIS REPORT
Client
Contact
CELANESE
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 2B152
Richard Ramirez
Client ID: V-23
Para.meter
Wet Chemistry
SW846 9060
Matrix
ORGANIC CARBON, TOTAL
: GW/Chemw
Result Qual
8900
NC Certification Number: 25
Project Number: 61621.01
Report Date June 15, 2005
Page 5 of 13 Report ID: AC1629
Sample ID L05050602-0l
Date Collected: 05/04/2005 0000
Date Received 05/06/2005
RDL Units Analyst Date Time
200 mg/1 CDC 05/18/2005 1630
I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-4413 I Fax (864) 229-7119
D~IS
FLOYD
Client
LABORATORY ANALYSIS REPORT
CELANESE
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
NC Cenijication Number: 25
Project Number: 61621.01
Contact Richard Ramirez
Report Date
Page 6 of 13
June 15, 2005
Report ID: AC1629
QC Summary Data
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I HJ 6 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-441 J I Fax (864) 229-7119 I
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DAYIS
FLtrYD LABORATORY ANALYSIS REPORT
Sample ID
L05050410-01
L05050410-02
MB41176:l
LCS41176:l
Client
Contact
CELANESE
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Richard Ramirez
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 7 of 13
June 15, 2005
Report ID: AC1629
QC Batch Report -Batch Sample List
WorkGroup WG41176 Matrix GW/Chemw
Description: TOC Prep Method
Analtyical Method: SW846 9060
PREP ANALYTICAL
Client ID •=• Date Time Date Time Analyst
K-28 1 05/13/2005 0819 CDC
DUP-2 1 05/13/2005 0923 CDC
Method Blank 1 05/13/2005 0551 CDC
Laboratory Control Spike 1 05/13/2005 1255 CDC
Dilution
1
1
I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-441 J I Fax (864) 229-7119
DAYIS
FLtffD LABORATORY ANALYSIS REPORT
Client
Contact
CELANESE
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Richard Ramirez
QC Batch Report -Method Blanks
Parameter
Wot Chemistry
SW846 9060
WorkGroup: WG41176
Blank MB41176:l
ORGANIC CARBON, TOTAL
Result Qual
1.0
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page a of 13
Matrix: GW/ChemW
June 15, 2005
Report ID: AC1629
RDL Units Analyst Date Time
1.0 mg/1 CDC 05/13/2005 0551
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Dav;, ,Hluyd, Inc. I PO Drawer 42/J I Greenwood, SC 2%48 I 816 E. Ducst Avenue I Greenwood, SC 29649 I (B64) 229-4413 I Fax (864) 229-7119 11
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DAYIS
FLtJYD LABORATORY ANALYSIS REPORT
Client
contact
CELANESE
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Richard Ramirez
NC Certification Number: 25
Project Number: 61621.01
Report Date
Page 9 of 13
June 15, 2005
Report ID: AC1629
QC Batch Report -Laboratory Control Standards and Duplicates
WorkGroup: WG41176 Matrix GW/ChemW
LCS LCS41176:l Prep Method
Analtyical Method: SW846 9060
ORGANIC CARBON, TOTAL 25.00 24.86 mg/1 99 90-110
I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-4413 I Fax (8641 229-7119
D~IS
FLtJfD LABORATORY ANALYSIS REPORT
Client
Contact
CELANESE
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Richard Ramirez
NC Cenification Number: 25
Project Number: 61621.01
Report Date
Page 10 of 13
June 15, 2005
Report ID: AC1629
QC Batch Report -Batch Sample List
WorkGroup WG41223 Matrix GW/Chemw
Description: TOC Prep Method
Analtyical Method: SW846 9060
PREP ANALYTICAL
Sample ID Client ID Run# Date Time Date Time Analyst
L05050602-01 V-23 05/18/2005 1630 CDC
MB41223:l Method Blank 1 05/18/2005 1455 CDC
LCS41223:1 Laboratory Control Spike 05/18/2005 2056 CDC
MS05050901-07 41223 Matrix Spike 1 05/18/2005 1957 CDC
MSD05050901-07:41223 Matrix Spike Duplicate 1 05/18/2005 2026 CDC
Dilution
200
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Davb & i:/oyd, Jnc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-4413 I Fax (864) 229-7119 I
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Dl\VIS
FLffl'D LABORATORY ANALYSIS REPORT
Client
Contact
CELANESE
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Richard Ramirez
QC Batch Report -Method Blanks
Parameter
Wet Chemistry
SWB46 9060
WorkGroup: WG41223
stank MB412231l
ORGANIC CARBON, TOTAL
Result Qual
< 1.0
NC Cenijication Number: 25
Project Number: 61621.01
Report Date June 15, 2005
Page 11 of 13 Report ID: AC1629
Matrix: GW/ChemW
RDL Units Analyst Date Time
1.0 mg/1 CDC 05/18/2005 1455
I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-4413 I Fax (864) 229-7119
DAYIS
FLtJYD LABORATORY ANALYSIS REPORT
Client
Contact
CELANESE
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Richard Ramirez
NC Certijica1ion Number: 25
Project Number: 61621.01
Report Date
Page 12 of 13
June 15, 2005
Report ID: AC1629
QC Batch Report -Matrix Spikes and Duplicates
WorkGroup: WG41223 Matrix GW/ChemW
M&/MSD MSOS050901-07:41223 Prep Method
MSD05050901-07:41223 Analtyical Method: SW846 9060
ORGANIC CARBON, TOTAL 20.00 9. 74 29.14. mg/1 97 74-125
ORGANIC CARBON, TOTAL 20.00 JO.OS 102 3 11 74-125
NOTE: MS/MSD, recoveries are not evaluated if the sample concentration is greater than four times the spike added.
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Davis & Floyd, Inc. / PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (804) 229-4413 I Fax (864) 229-7119 I
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Dl\VIS
FLtrYD LABORATORY ANALYSIS REPORT
Client CELANESE
2525 BLACKSBURG ROAD
HWY 198
SHELBY, NC 28152
Contact : Richard Ramirez
NC Certification Number: 25
Project Number: 61621.01
Report Date June 15, 2005
Page 13 of 13 Report ID: AC1629
QC Batch Report -Laboratory Control Standards and Duplicates
WorkGroup: WG41223 Matrix GW/ChemW
LC!S LCS412231l Prep Method
Analtyical Method: SWB46 9060
ORGANIC CARBON, TOTAL 25.00 26.22 mg/1 105 90-110
I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2%48 I 816 E. Durst Avenue I Greenwood, SC 29649 I (ll64J 229-4413 I fax {864) 229-71 19
DA,YIS
FLtJYD LABORATORY ANALYSIS REPORT
Method Conformance Summary
Client Celanese -Ticona, LLC, Shelby Plant
Login(si L050504 I 0, L05050602
Criteria TOC
Sample Holding Time ✓
Standards Preparation ✓
Instrument Tuning ✓
Instrument Calibration ✓
Calibra;ion Verification ✓
Degradation Check NIA
Interference NIA SamolelStandard
Blanks Results ✓
Method Accuracy ✓
Method Precision ✓
Surrogate Recovery ✓
PDSISDIMSA NIA
TCLP Preparation NIA
Key ✓ Method Criteria Met
NIA Not Applicable
• = Method Criteria Not Met -Seefootnote(s) below.
PDS = Post Digestion Spike
SD = Serial Dilution
MSA = Method of Standard Additions
Footnotes:
Prepared by: ____________ _
Project Number: 61621.01
Report Date: June 15, 2005
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D.1vis 8, Floyd. Inc. I PD Drawer 42H I Greenwood, SC 2%411 I H 16 E. Durst Avenue I Creenwood, SC 2%49 I (llf,4) 229-4411 I Fax JH!,4) 229-71 191
-~-- - - - - - - - --SHEALY ENVIRONMENTAL SERVICES, INC. '-.
S V Ch · f C t d R d 106 Vantage Point Drive · ,I Bin O US O Y eCOf Cayce, South Carolina 29033
J5 ✓ J.5-,~'tY Telephone No. (803) 791-9700 Fax No. (803) 791-9111
"'50~~1cr
Number 16850 -
Ghent f:.ug,.j{-Mt', ·tk...Ioc (,(725" Report to Contact ej2, . j::::,,.'~j Q{~ ~'7 u. l. T~hone No.! fax N~. IE-~ . ~-P?2 ·-M9o. f&v-fl:2.-.Jl&J
Quote No.
Address ·fa fidY ~Ir) 'f 7 S~tuce. ·~
Waybill No. '
Page 1 o,L
c;,'.;1,t1-tff"t1NV/1.,,lt: 1. State I Zip Code. , V :Z.,'~.A 7. Analysis (Attach list if more space is needed.) -\
.Sc ;;27£,,J--c, ..
Printed Nt,> /
PmjectName c•;u4-)t/C,{J,t//f 6 ~ 7.,--01?._7 T;~t/£.4,/pJ 1;( Project No. bLbOS/b P.O. No. ~ I No. of Containers Lot No.
!i Matrix by Prese,vative Type
Sample ID I Description Date Time l . • 0 M ~ J <:~ ~ Is (Containers for each sample may be combined on one fine.) , I ~ ~f § ~ \l ~ 8 Remarks I Cooler 1.0. < < ~
~-:}<Y 3/'l/4s' OJ~ Co X I X <->czr~,c cl720c:
(35c I / 'I~ .r V I • ✓
,if== j htf!S I{:, V V _} .,, . I /\
007-62. -G X: I X
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OA.J 'T/1: Jb»,4-f'J
7;1~ Jt?,2.J
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Possible Hazard fdentif1CB.tion □ Skin lrrita/,,6~ison
Sample Disposal Note: All samples are retained for six weeks from receipt
□ Non-Hazard □ Rarpmpble □ Unknown □ Retum to Client L'£Disposal by Lab unless other arrangements are made.
Tu~ Aroun~ ~12d (Pnor lab apptl re'quired for expedited TAT)
rhtStandard u.c,J,i· (Specify) , /
'oc Requirements (Specify)
LGVL~ :JI:.
/t. Rehngu~tfy ';//:_ --Dateto//4 Ti/(/?,) 1.-~nv~ I>~ 0 a::z , Time /' lffi-e:-~ -------S; ,,,-~ 14 '?lJ -< 2.TL~is ed~d'-:) / 0
"'/1 in, Time 2. ReceivtJI,, y Date Time ,., .'11Y s 'i -l(,3n
3. Relinquis. Mby Date Time 3'"tis'o;.'ec5-b'w-, '-(;,C0J { ':%. I/. 05
Time 1&:3-o
Comments LAB USE ONLY e~ rJ Received on ice (Circle Yes Jee Pack Receipt Temp. "C
DISTRIBUTION. WHITE & YELLOW Return to laboratory with Sample(s), PINK F1e/d/C/lent Copy '--
61f-,
ui:rl.LY Chain of Custody Record
,J-t'ft-,,yb
Sample ID I Description
(Containers for each sample may be combined on one line.)
l/✓23 .
/I
PO. No.
Date
I '
Possible Hazard Identification / /
□ Non-Hazard □,Flammable □ S,J<in lrrit,y,t □ Poison □ Unknown
-~ Tu11 Around Tjme V/equired (Prior 1,f> BPP(OVa! required for expedited TAT.)
M Standard ~ush (Specify) /,1. /
SHEALY ENVIRONMENTAL SERVICES, INC.
: 06 Vaniage Point Drive
Cayce, South Carolina 29033
Telephone No. (803) 791-9700 Fax No. (803) 791-9111
Waybill No.
• No. of Containers
o" Matrix by Preservative Type lH
Time "0 i " ~ i Ii ~ ~u };: <:~ 8 ~ " ~ u 0 ~, ~ ! ~ 0 "' ._ ~ 0 s 0
(; X I IX
L 0...5 ·os-o& o i
Number 15·3 4 8
Quote No.
( I
Page of-----+-
.. Analysis (Attach list if more space is needed.)
Lot No.
Remarks I Cooler 1.0.
fcrAri: ltft.e.,1 /tti
·llG VBJJ /fl.,;1,u
1/fd' ?J,o:;-zz.T,.,, Jb04)
/,?v 7?/c )btiJ.97
Sample Disposal
□ Return to Client ( Disposal by Lab
Note: All samples are retained for six weeks from receipt
unless other arrangements are made.
/ QC Requirements (Specify)
-I
5.~o5 Tfrn•o1..3 0
lAB USE ONLY
Received on ice (Circle~ No Ice Pack Receipt Temp. .1!.. - ---
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Kubal·Furr & Associates Project No. 2(; QS. {(z / Z6 .VA 'ii. ' -[m,iro111111•11f11/ C1m~1i//1111/~ -Site Loco lion CNA/Ticona -Shelby, NC
Field Personnel gs .
Well I Sample 10 -..f-..~-~2_~'>?~-~-~-c:,· i [! ~ Wea/her Conddion Si,,)'t'.1/~ ~5 5d S Sample Dale --~--'--;/c=../==,---;__:A;::;•ri;,:;;,a;::;I Tim;::;e~ _o_•rrc,_•_,....::.:Sa;::;mp:_:ie:_.::rim:_.::e~ -~(_~1 "';~=:-.f:,=c===,--
Descrip!1on of ,\temuringl ·/eel. ii cc,·,ng T'/pe! (). r•· 11' L-:::cking Cop! / ,! Cosingll ~ i Pcint (MPJI , I rvL c,cme:e1 ,nehei• ::===:::.,_.. _ __;-~~ PvrgeMerhodl ~¼H,\L.-; SomplingMetr",ed/ ~-,,¼J.l-\L I __
Purg'! ':,t~rl [imell 'ooq-i ' PUP;;!<? $loo fime; iD>D j Purge .~ot<:,\.1.,./ /'i.11m.nl
Waler-Level Measuremenls Field Parameters
fm'1ru) . -(~Cl (~iiL') ~q, (µ$/cm)
ln!erval Elapse lime DTW U""et) lnt.,.rval Temperature Speciric Conductance pn (;vJ T\:rt,oity ORP (m\l)
0 I 0 I !s't I 0 I I I I I ' I ' ' I -· I 1'-/S'i~ I 1'5.?o 1 sL/ci I 6, 7,4 I I 3, I z.;,; I _.:..k'c,, /'. I '() I
2 I lo liJ I') g 2 I 15, ~-~ I zdff I I. "'J? I ;7 I z.s-!-i'G,.3
3 I is-!rs. sci 3 I /r;<-',1 s 4) i r. s 3 I l 5 I 1...u [ -7Z< ' I 1o ii S, 5'2 4 I /5,C/ t I 543 ! (_, 3/ I 1 '1 I I,') I-'it/, 5 I ,z,r I !5,7'-i 5 I Jl,. ai./ I 3 L/ I i r . )0 I ·7 r,, I 17.... 1-'1(, Z I YJ I J'J,C/1 I I I., /2-' '?L/0 I r,,, z 'l I 7 0 I I, ':> l-917 I 6 6 I
7 I J,'5 f ,c,_ifi 7 ! /(,, ZJ) ! '.>3'6 I (,,, ZY 137 i 1, r 1-81,7
8 I 4o I ;1o,z1 8 \ 11., l'i I )3G 1. (.,, Z'i, 13 S' I I • l /-fr.ti I 9 I /.fS-I 17 co ' 11&, 24 ! 3 31 I c,,27 1:s"I I J ,o l-tg,1
10 I <;""() ! 17, 70 10 l/fc.17 I ~11 i /,-L llL!t'i I I ,c> f-f'U :S ' II I II I ! I I I 12 I " I ! I I I 13 I 13 I I I I I I /4 I I /4 i I I I I I 15 I I 15 I I I I I I 16 • I I 16 I ! I I I I I
17 I I 17 I I ! I I I I
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Samples Collected Con101ner Descnp,1on ,.
( X iZ5 inL
· j_~:;(cR 1u2::..)2.1 N101~ luff-l~<i
R,H-::. zdlcJ:fcf(Y\ > z./.0"'1/L
T~rbidi:y +/-IC;; ot>ove 10 NTU +/-I NTU below 10 ,'lTU Oi?P +/• ICmV Ccr,.ve-s;M fa~,
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Low-FlowGroundwoler Sompijng tog
Kubal-Furr & Associate:;
-[11t•iiw1111t·irMI C1m,11/tmrl:;-
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10 I 10
II I II
12 I I 12
13 I I 13
" I " 15 I 15
16 I 16
17 I I 17
18 I I 18
19 I I 19
20 I 20
Somples Collected
Low-Flow 'crour,cwcter Sampling Leg
P.·ojectNo 2 l°'s I l (2(,)/1.//1. 9'7
Site Location CNA/Ticona -Shelby, NC
Field Personnel ~-,{.l,'--=5'-.--c------
We/1 I Sample ID ---cc✓~-=l~s--,,-.,._-,-c=----
S J:,, ~ G,O's
/
', ,wzel·therCor.aition ~,~~""'·7'-'.-'--1-+-'~---'1 "' Somo:, T,me _::, .:,__
µ cm
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forbidity
(,'ITU)
I 1038' ! 4/•7/ I Lf. x'7 I '-I (c
Ii/.. 30 I r/20>1 1 'lo i S.& 1 /tc?"7 : i/Zo 7 I 4, °I u I L-1.'-
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Container D~npt,on Prese1Va1.ve
*Dis,olvcd
o~ygen ORP (mV) ~.,. '-.C,
' ' ' I
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low-flowGro,..ndwoter Somp:ir,g log
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I Attachment 2
I Selected Water-Quality Plots
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I Kubal-Furr & Associates
-------------------
:::,
V-23 TOC Data
14000 ,---------------------------------------------~
(Unfilled data points represent qualified data
or values below the detection level.)
12000 -- ------ - ---- - ----- - -- --- - - ---- - - ------- --- ------- - - ------- - - --------- -- ------ --------- - -------- -- - ------
10000
'o, 8000 E ~
5 -~
~ g 6000
8
4000
2000
0-t-----+------+-------t-~------+------+-----+-----1-------+--_J
1/1/85 6/20/87 12/6/89 5/24/92 11/10/94 4/28/97 1 0/1 5/99 4/2/02 9/18/04
Date
-------------------
C 0 ~ 1:: 8 C
8
V-23 2-Butanone (MEK) Data
4,--------------------------------------------~
3.5
3
2
1.5
0.5
(Unfilled data points represent qualified data
or values below the detection level.)
---- ---------------- --- ----------------- -------- --------- --- --------- ----- - - - ---------- --- ------------
---------------------------------------- --------------------------------------------------
-------------------------------------------------------------------------------------------------
0 +----"'---0----t.,,._,,'--------'=--+-""0----0-+----~::.-----+-----t----------+'ID--O--O--B-+-__J
6/1 /89 6/1/91 5/31/93 5/31/95 5/30/97
Date
5/30/99 5/29/01 5/29/03 5/28/05
-------------------
V-23 Acetone Data
1.4-,---------------------------------------------~
1.2
0.4
0.2
(Unfilled data points represent qualified data
or values below the detection level.)
0+---~~+------+--'-'---_.'+-----+-~-__[J4--------+-----f-O===i~~,E)_+---__J
6/1 /89 6/1/91 5/31/93 5/31/95 5/30/97
Date
5/30/99 5/29/01 5/29/03 5/28/05
-------------------
~ ..J ' "' E ~
C 0 .,
E .,
C Q) u C 0 u
V-23 Benzene Data
0.3 ,-------------------------------------~
0.25
0.2
0.15
0.1
0.05
(Unfllled data points represent qualifled data
or values below the detection level.)
--------------------------------------------------------------------
---------------------------------------------------------------------
------ - - -------- ---- -- --- - -- -----------------------------------
------------------------------------------------------------------------
0 -t------+-----+=-----+----+------+----+------t:1---------+----+.----I
6/1/89 6/1/91 5/31 /93 5/31/95 5/30/97
Sample Date
5/30/99 5/29/01 5/29/03 5/28/05
-------------------
'.J' -;,,
K-28 TOC Data
9000 ~-------------------------------------~
(Unfilled data points represent qualified data
or values below the detection level.)
8000 ------------ - ----- - -- - - -------- - - - - ------- ------- -- ------ -- - --- - - ----- - ------ - -
7000 -- ------ ---- - - --- - -- - - - - - -- ---- -- -------- -- - ------ -. ------- ----- -- - - ----- - - ------------- ---------
6000
_§, 5000
C: 0 ~ e ~ ~ 4000
8
3000
2000
1000
0 +-------+-------l-----+------+-____:o,. .... ~-~ ............ --~-----1+-11.J-------~
8/14/81 8/18/84 8/23/87 8/27/90 8/31/93
Date
9/4/96 9/9/99 9/13/02 9/17/05
-------------------
C 0 .,
E ~
K-28 Benzene Data
0.035 ,----------------------------------------------~
0.03
0.025
(Unfilled data points represent qualified data
or values below the detection level.)
g 0.01 5
0 u
0.01
0.005
0+------+--------1-----+------+-----t--------+-------+-----+---_J
6/1/89 6/1/91 5/31/93 5/31 /95 5/30/97
Date
5/30/99 5/29/01 5/29/03 5/28/05
-------------------
C 0 .,
~ C .,
u C
HH-48 TCE Data
0.25 ,-----------------------------------------------~
0.2
(Unfilled data points represent qualified data
or values below the detection level.)
8 0.1
0.05
0+------------+-----+------l--------+------+------+------e--J
6/30/89 6/30/91 6/29/93 6/29/95 6/28/97
Date
6/28/99 6/27 /01 6/27/03 6/26/05
-------------------
HH-77 TCE Data
0.5 -,------------------------------------------~
0.45
0.4
0.35
(Unfilled data points represent qualified data
or values below the detection level.)
-------------------------------------------------------------------------------------------
---- ---------- - - ------ -- - - - ------ --- ---- -------- -------- ------ - -----
----------------------------------------------------------------------------
C 0 -~ 0.25 ..,
C fl C 8 0.2
0.15
0.1
0.05 ---------------------------------------------------------------------
0+------+-----t-----f--------1-----+------+-----+------+__J
6/1/89 6/1/91 5/31/93 5/31/95 5/30/97
Date
5/30/99 5/29/01 5/29/03 5/28/05
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I Attachment 3
I CD ROM of Semiannual Report
In pdf Format
I (Back Cover)
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I Kubal-Furr & Associates