NCD003446721_20010313_Celeanse Corporation - Shelby Fiber_FRBCERCLA RA_OU-1 Semiannual Report July - December 2000-OCR

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Operable Unit 1-Semiannual Report
July 2000 -December 2000
CNA Holdings, Inc.
Shelby, North Carolina
(F.K.A. Hoechst Celanese Corporation)
Document Control No. 0265B-0095
Submitted to
U.S. Environmental Protection Agency
Region IV
Atlanta, Georgia
_
0 Prepared for
CNA Holdings, Inc.
Shelby, North Carolina
March 2001
Kubal-Furr & Associates
SUPERFUND SECTION
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Kubal-Furr & Associates
-----------Environmental Management Services
Post Office Box 273210
Tampa, FL 33688-3210
[phone]
FAX [phone]
[e-mail]
Mr. McKenzie Mallary
Remedial Project Manager
U.S. Environmental Protection
Agency, Region IV
100 Alabama St., S.W.
Atlanta, GA 30303-3014
Dear Ken:
March 13, 2001
Post Office Box 80247
Simpsonville, SC 29680-0247
[phone]
FAX [phone]
[e-mail]
On behalf of CNA Holdings, Inc., we are pleased to enclose two copies of the report entitled:
"Operable Unit I-Semiannual Report-July 2000-December 2000-CNA Holdings,
Inc.-Shelby, North Carolina." By way of this letter, we have also transmitted a copy of the
report to Bruce Nicholson with NCDENR for his review.
Please get back with either Mr. Jerry McMurray at 704-480-4656, or me at 813-265-2338, to
discuss any questions you may have following your review of this document.
Sincerely,
Kubal-Furr & Associates
~ilt,0-f_
Jerry E. Kubal, P.G.
Presi&nt
cc: Mr. Bruce Nicholson, NCDENR
Mr. Jerry McMurray, Ticona-Shelby ESHA
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Contents
Page
Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Work Performed . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
3rd Quarter 2000 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
4th Quarter 2000 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
System Performance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Inner Tier Extraction Rates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Ground-Water Movement .............................................. 4
Treatment Efficiencies . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
Maintenance Activities . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Analytical Test Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Data-Quality Assessment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Discussion of Analytical Test Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Review of Selected Historical Water-Quality Data . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Closing Comments . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
Table 1.
Table 2.
Table 3.
Table 4.
Table 5.
Table 6.
Tables
2000 Sampling Matrix-CNA Holdings, Inc.-Shelby, NC
Inner Tier Production Data (July 2000 -December 2000)
Inner Tier TOC Data (July 2000 -December 2000)
Summary of Selected CERCLA-related Water-Quality Data (3rd Quarter 2000)
Summary of Selected CERCLA-related Water-Quality Data (4th Quarter 2000)
Summary of Selected PEW-related Water-Quality Data (3rd Quarter 2000)
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Figures
Figure 1. Site Plan Showing Monitoring Locations and Geologic Cross Sections
Figure 2. Potentiometric Surface Map-Shallow Saprolite-July 18, 2000
Figure 3. Potentiometric Surface Map-Deep Saprolite/Upper Bedrock-July 18, 2000
Figure 4. Hydro geologic Cross Section A-A', July 18, 2000
Figure 5. Potentiometric Surface Map-Shallow Saprolite-October 24, 2000
Figure 6. Potentiometric Surface Map-Deep Saprolite/Upper Bedrock-October 24, 2000
Figure 7. Hydrogeologic Cross Section A-A', October 24, 2000
Attachments
Attachment 1. Operation and Maintenance Data (July 2000 -December 2000)
Attachment 2. Analytical Data for the July and October 2000 Sampling Events
Attachment 3. Selected Water-Quality Plots
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CNA Holdings, lnc.-Shelby, NC-Semiannual Report/Page I
Introduction
CNA Holdings, Inc. (formerly known as Hoechst Celanese Corporation) is currently operating
a long term remedial action (LTRA) system at its Shelby, North Carolina facility. This system,
designated as Operable Unit 1 (OU-1) in the Record of Decision (ROD), consists of two ground-
water extraction and treatment systems identified as the Inner Tier and Outer Tier systems. OU-1
became operational in August 1989.
On April 21, 1998, the Outer Tier portion of OU-1 was shut down as part of a partial delisting
petition approved by the EPA effective April 17, 1998. Active ground-water recovery and treatment
is currently only taking place at the Inner Tier which was designed to extract contaminated ground
water from around a former source area remediated as a separate operable unit (OU-2) with its own
ROD. Although the Outer Tier is not actively recovering ground water, Outer Tier well OT-lR is
still pumped to provide make-up water for the SBR (sequencing batch reactor) and for process
water used for backflushing filters. The entire Outer Tier is being maintained in "stand-by status"
as part of the delisting process and can be brought on line within a relatively short period of time
(24-48 hours) if it is found necessary to provide hydraulic control along the property boundary.
Kubal-Furr & Associates has prepared this semiannual OU-1 operating summary report for
submittal to the EPA on behalf of CNA. It covers the period from July 1, 2000 through December
31, 2000 and includes information on system performance and the results of analytical testing of
samples collected on July 19, 2000 and October 25, 2000.
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CNA Holdi11gs, /11c.---Shelby, NC-Semia1111ual Report/Page 2
Work Performed
As part of the OU-1 remedy, samples are collected at selected monitor wells and at points in the
ground-water treatment system. In addition, samples were collected from the PEW extraction well
system and PEW-related monitor wells. A list of sampling locations and the parameters analyzed
during the 3rd and 4th Quarters are summarized in Table 1. A description of the work performed
during this reporting period is provided below.
3rd Quarter 2000
On July 18, 2000, water levels were measured by Kubal-Furr in a total of 95 monitor wells,
extraction wells, and piezometers. A total of 17 water-quality samples, 2 duplicate samples and one
field blank were collected on July 19, 2000 from selected monitor wells and extraction wells.
Additionally, 2 process point samples were collected. All samples were collected and analyzed by
Davis & Floyd of Greenwood, South Carolina.
OU-1 Monitor Well Sampling
Thirteen monitor well samples (plus 1 duplicate) were analyzed in the field for pH, temperature
and conductance; and, by the laboratory for volatile organics (VOCs) using EPA Method 8260B.
Samples from monitor wells K-28 and V-23 were also analyzed by the laboratory for TOC using
EPA Method 9060.
OU-1 Process Point Sampling
Samples of Inner Tier influent and effluent were collected for analysis of volatile organics by
Method 8260B. The Inner Tier influent and effluent samples were also analyzed by the laboratory
for total organic carbon (TOC) by Method 9060, and for ethylene glycol by GC/FID.
During the reporting period, influent and effluent samples from the Inner Tier were also
collected by CNA personnel for analysis of TOC by Davis & Floyd. These samples are collected
weekly to evaluate treatment efficiency, and the results are contained in the O&M reports provided
in Attachment 1. These results are also summarized in Table 3.
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CNA Holdings, Jnc.--Shelby, NC-Semiannual Report/Page 3
PEW Extraction and Monitor Well Sampling
One PEW-related monitor well (F-55) and 3 PEW extraction well samples (plus 1 duplicate)
were collected during the 3rd Quarter. These samples were analyzed for VOCs by EPA Method
8260B and for SVOCs (semivolatile organics) by EPA Method 8270C (including biphenyl and
diphenyl ether).
4th Quarter 2000
On October 24, 2000, water levels were measured by Kubal-Furr in a total of 91 monitor wells,
extraction wells, and piezometers. Water-quality samples were collected from 2 process points and
2 monitor wells (plus one monitor well duplicate) and analyzed for the parameters summarized in
Table 1. The samples were collected on October 25, 2000 by Davis & Floyd, who also performed
the analyses.
Monitor Well Sampling
Monitor wells K-28 (and K-28 duplicate) and V-23 were sampled during the 4th Quarter
sampling event. These wells were analyzed in the field for pH, temperature and conductivity; and, by
the laboratory for TOC by Method 9060.
Process Point Sampling
Samples of Inner Tier influent and effluent were collected for analysis of TOC by Method
9060 and volatile organics by EPA Method 8260B. The Inner Tier influent and effluent samples
were also analyzed for ethylene glycol by GC/FID.
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CNA Holdings, lnc.--Shelby, NC-Semiannual Report/Page 4
System Performance
Detailed records of system maintenance are kept by CNA and are summarized monthly. The
monthly records for the current reporting period are contained in Attachment 1. Summaries of
physical operating data for the Inner Tier extraction well system is presented in Table 2.
Inner Tier Extraction Rates
During the reporting period, the Inner Tier wells extracted a total of 236,438 gallons. Inner Tier
flows ranged from a low of 35,443 gallons in August, to a high of 41,646 gallons in July. Pumping
from the Inner Tier wells is limited by the capacity of the SBR treatment system, which is designed
to process about 2500 gallons of water per day. With 184 days in the reporting period, at design
capacity, pumping from the Inner Tier would have been some 460,000 gallons. Based on the
pumpage during the reporting period, the Inner Tier extraction system was producing at a rate of
about 51 % of the design capacity, which represents a decrease from the previous semiannual
reporting period during which the Inner Tier produced about 64% of the design capacity rate.
The continued decline in production from the Inner Tier has been discussed in detail in the draft
Five-Year Review Report submitted to the EPA in December 1999. This report is still under review
and no action has been taken with regard to recommendations made concerning Inner Tier
pumpage.
Ground-Water Movement
In order to accurately predict the direction of ground-water movement, water-level
measurements were collected from all accessible monitor wells, extraction wells and piezometers on
July 18, 2000 by KF&A, and again on October 24, 2000. These data were used to construct the
potentiometric surface maps and hydrogeologic cross sections (Figures 2 thru 7).
The shallow saprolite maps (Figures 2 and 5) show the water-level contours and direction of
ground-water movement in the uppermost water-bearing zone beneath the site. The direction of
movement in this zone is to the east from upgradient areas along NC 198, towards discharge areas
along the intermittent, unnamed tributaries of Buffalo Creek. Drawdown and a capture zone are
apparent on these figures situated around the Inner Tier extraction system.
An attempt was made to separate the uppermost water-bearing zone from the deeper saprolite
and upper bedrock zone. While these maps (Figures 3 and 6) present a reasonable picture of
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CNA Holdings, lnc.-Shelby, NC-Semiannual Report/Page 5
ground-water movement in this zone, it should be pointed out that it is giving a somewhat more
generalized picture of ground-water movement because of the well construction techniques used in
many of the wells and piezometers. The typical construction of these wells was to have relatively
long screens (20-40 ft) and extremely long sand packs in the annular space above the screens (up to
60-ft). As a result, the lower saprolite/upper bedrock maps have a number of composite head values
measured along a longer screened area. However, the maps may be useful for determining the
general direction of ground-water movement.
To confirm inferences made about the direction of movement and hydraulic control exerted by
the Inner Tier system, hydrogeologic cross sections were constructed from the July and October
data sets (Figures 4 and 7). The location of the cross section is shown on the site base map, Figure
1. The east-west cross section (A-A') is constructed through the plant from upgradient areas west
of the plant to downgradient, off-site areas east of the plant. The east-west hydrogeologic cross
section shows a general direction of movement in the saprolite and upper bedrock from upgradient
areas west of the plant toward downgradient areas to the east. No appreciable downward hydraulic
gradients are apparent on this map, and the movement in the saprolite and shallow bedrock is
predominantly horizontal across the site.
Treatment Efficiencies
Two aspects of the extraction system performance were reviewed for this semiannual report: the
production rates achieved during the reporting period, and the removal efficiencies for TOC from
the Inner Tier system.
Taqle 3 summarizes the treatment system effectiveness for the Inner Tier in removing TOC
during the reporting period. These summaries were prepared from the water-quality data collected
weekly by the CNA on-site laboratory as presented in the monthly operating summaries
(Attachment 1). During the reporting period, the Inner Tier average removal efficiency for TOC was
greater than 98%, with an average influent concentration of 1662 ppm (parts per million), and an
average effluent concentration of 25 ppm. While the TOC removal efficiency was generally greater
than 99% during the first half of the reporting period (i.e., the 3rd Quarter), it generally remained
below 98% during most of the 4th Quarter and typical effluent concentrations for TOC were
notably higher in the 4th Quarter versus the 3rd Quarter.
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CNA Holdings, lnc.-Shelby, NC-Semiannual Report/Page 6
Maintenance Activities
Low flow from the Inner Tier wells is a chronic problem requiring frequent maintenance. The
actions taken to rectify the low flow problems consisted of replacing bladders, timers, air lines and
such, adjusting the controls and flow rates, and cleaning the strainers. Specific actions taken at
individual wells during the reporting period are contained in the monthly operating summaries
(Attachment 1).
Kubal-Furr & Associates
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CNA Holdings, lnc.-Shelby, NC-Semiannual Report/Page 7
Analytical Test Results
The analytical test results for the 3rd and 4th Quarter sampling events were evaluated using
method specific quality control criteria and, for additional guidance when necessary, the EPA's
National Functional Guidelines for organic and inorganic data review. The data assessment
summary sheets, analytical test results, field sampling logs, and chain-of-custody forms for the 3rd
and 4th Quarter data sets are contained in Attachment 2. A summary of selected analytical data for
the 3rd and 4th Quarters is presented in Tables 4, 5 and 6.
Data-Quality Assessment
All 3rd and 4th Quarter data were considered Class A (quantitative) with the following
exceptions:
•
•
During the 3rd Quarter, results for ethylene glycol exceeded the calibration range during the
initial analysis of sample ITCI. The sample was diluted and reanalyzed out of holding time.
Results from both analytical runs were reported by the laboratory and qualified as
estimated. These results were flagged with a "J."
During the 4th Quarter, acetone and 2-butanone were detected in the trip blank. Positive
results for acetone and 2-butanone in the associated samples at levels less than 10 times that
found in the trip blank were flagged with "U" and the reporting limit raised to the
concentration of acetone or 2-butanone present in the sample. The only associated sample
containing acetone or 2-butanone was ITCI. Results for these compounds in ITC! were
flagged as indicated above.
• Also during the 4th Quarter, the relative percent difference between sample K-28 and the
field duplicate sample K-28 Dup. was outside acceptance criteria for TOC. Results for TOC
in K-28 and K-28 Dup. were flagged with "J."
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CNA Holdi11gs, lnc.---Shelby, NC-Semia1111ua/ Report/Page 8
Discussion of Analytical Test Results
CERCLA-Monitor Wells
Of the 13 CERCLA-monitor well samples analyzed during the reporting period, only five had
any volatile organics reported above the detection level (Tables 4 and 5). Of these six, only one (V-
23) had more than one individual volatile constituent reported as present above the detection level.
Monitor well V-23, located downgradient of the former OU-2 source area and just upgradient
of the Inner Tier extraction system, reportedly contained acetone (0.47 mg/L), benzene (0.021
mg/L), 2-butanone (0.42 mg/L), and carbon disulfide (0.041 mg/L). Monitor wells HH-48 and
HH-77, off-site and adjacent to the Elliott residence, reportedly contained trichlorothene (TCE) at
concentrations of 0.072 mg/Land 0.14 mg/L, respectively. The presence of TCE at this location is
thought to be the result of a localized source, unrelated to activities at CNA or the former OU-2
source area.
Monitor wells K-28 and V-23 were also analyzed for TOC during the 3rd and 4th Quarters.
The V-23 test results for the 3rd and 4th Quarters were 11700 mg/Land 10800 mg/L, respectively.
The TOC test results for K-28 were noted to increase from 16.7 mg/L to 163J mg/L between the
3rd and 4th Quarters. As previously noted, the K-28 4th Quarter result has been flagged with a "J"
as estimated because the RPD between the sample and duplicate were outside acceptance criteria.
Process Point Samples
Inner Tier influent and effluent samples were analyzed during the 3rd and 4th Quarters for
ethylene glycol, TOC, and volatile organics. All volatile test results for the Inner Tier effluent
sample were below the detection level during both the 3rd and 4th Quarters. Ethylene glycol for the
Inner Tier effluent sample during the 3rd and 4th Quarters were reported below the detection level
of 7.0 mg/L. Inner Tier effluent TOC was reported as 12 mg/Land 25.9 mg/L for the 3rd and 4th
Quarters, respective! y.
The 3rd Quarter Inner Tier influent sample reportedly contained the volatiles acetone (0.13
mg/L), benzene (0.029 mg/L), chlorobenzene (0.02 mg/L) and carbon disulfide (0.052 mg/L). The
4th Quarter Inner Tier influent sample reportedly contained the volatiles benzene (0.013 mg/L) and
chlorobenzene (0.013 mg/L). Inner Tier influent ethylene glycol results for the 3rd and 4th
Quarters were reported at 802J mg/Land 779 mg/L, respectively. As previously noted, the 3rd
Quarter TOC result was flagged with a "J" as estimated because the sample was run out of
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CNA Holdings, /nc.---Shelby, NC-Semiannual Report/Page 9
holding time. Inner Tier influent TOC results for the 3rd and 4th Quarters were reported at 1580
and 1020 mg/L, respectively.
PEW-Related Samples
Of the four PEW-related samples collected during the 3rd Quarter, only F-55 and PEW-4 had
more than one volatile or semivolatile constituent reported as present. The volatiles acetone (0.021
mg/L), benzene (0.054 mg!L) and 2-butanone (0.015 mg/L) were reported as present in well F-55.
Cis-1,2-dichloroethene (0.008 mg/L) and trichloroethene (0.053 mg/L) were reported as present in
PEW-4.
Two of the four wells sampled had reportable quantities of Dowtherm constituents (i.e., 1,1-
biphenyl or biphenyl ether). 1,1-biphenyl was reported as present in wells F-55 (101 mg/L), and
PEW-4 (0.012 mg/L). Biphenyl ether was reported as present in well F-55 (292 mg/L) and PEW-4
(0.041 mg/L). Well F-55 also reportedly contained the semivolatile constituents dibenzofuran (0.34
mg!L), naphthalene (0.71 mg/L), phenol (0.058 mg/L), and 4-methylphenol (0.11 mg!L).
Review of Selected Historical Water-Quality Data
Attachment 3 contains plots of selected water-quality constituents for various monitor wells and
process points. The choice of locations and constituents was based on a review of the water-quality
database, in particular those locations having any meaningful data to plot. In general, only those
monitoring locations within a few hundred feet of the former OU-2 source area have any significant
number of water-quality constituents reported above the detection limits. In an attempt to assess
long-term improvement in water-quality conditions resulting from source removal and ground-water
recovery, the following locations and constituents were selected:
• Inner Tier Combined Influent TOC and ethylene glycol test results. The Inner Tier TOC
decreased from the 2nd to 3rd Quarter and between the 3rd and 4th Quarter. The Inner Tier
ethylene glycol data showed a similar response during the 3rd and 4th Quarters although no
long-term trends have been established.
• Monitor Well V-23 TOC, 2-butanone (MEK), acetone and benzene. The V-23 TOC data
began trending downward from a high of 8000 mg/Lin mid-1989 to less than 1000 mg/Lin
early 1992. Since that time, the TOC data have shown several wide swings in concentration.
TOC concentrations at V-23 increased during the 3rd Quarter and declined slightly during
the 4th Quarter.
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CNA Holdings, /nc.-Shelby, NC-Semiannual Report/Page JO
The V-23 MEK data have generally fluctuated in a narrow range below 1 mg/L, with 11 of
30 data points below the detection level. The values for MEK increased between the 3rd and
4th Quarter sampling events but no discernable trend is apparent in the data set.
The V-23 acetone test results have generally fluctuated in a narrow range below 0.6 mg/L
since 1989. Acetone concentrations at V-23 have been trending upward the past two years
and increased from below detection in the 1st Quarter of 1999 to above 0.40 mg/L during
the 3rd Quarter of 2000.
While more than half the benzene data for V-23 is flagged as estimated or below the
detection limit, the past 11 sampling events have been quantitative and show benzene to be
fluctuating in a narrow range of from 0.01 to 0.03 mg/L.
Monitor well K-28 TOC and benzene data. TOC and benzene have both shown a stairstep
decrease in concentration beginning about the time the OU-2 source remediation began in
January of 1991. An increase in TOC concentration was noted during the 3rd Quarter but
these data have been flagged with a "J" as estimated. Benzene at K-28 has remained
relatively stable at 0.01 mg/L since the 1st Quarter of 1999.
Monitor well HH-48 and HH-77 TCE data. The HH-48 TCE test results have declined
from a concentration of 0.222 mg/L in August of 1995, to 0.072 mg/L during the most
recent quarter (3rd Quarter 2000). HH-77 had been fluctuating in the range of 0.05 to 0.15
mg/L until the July 1996 sampling event when it peaked at 0.383 mg/L. TCE at HH-77 has
generally been trending downward the past four years from its high of 0.383 mg/Lin the
3rd Quarter of 1996 to 0.14 mg/Lin the 3rd Quarter of 2000.
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CNA Holdings, lnc.---Shelby, NC-Semiannual Report/Page I I
Closing Comments
The extraction well production data and the analytical test results for the monitor wells and
process points were generally found to be consistent with historical information, and no unusual or
unsuspected contamination was identified during the reporting period. Treatment efficiencies at the
Inner Tier for removal of TOC remained consistently greater than 98%, and no volatiles were
detected in either the 3rd or 4th Quarter Inner Tier effluent samples.
The next CERCLA-sampling events are scheduled for the 1st and 2nd Quarters of 2001, with
another PEW-related sampling scheduled for the 1st Quarter. The next scheduled semiannual
report is to be submitted to the agency by September 1, 2001.
Kubal-Furr & Associates
liiii ----
Monitoring
Location
Process Points
rm
ITEF
om
01EF
SBA Sludge
FP Sludge
Monitor Wells
C-49
K-28
P-58
T-35
V-23
AA-54
CC-33
EE-58
FF-34
FF-62
GG-61
HH-48
HH-77
TOC
(9060)
✓
✓
-------
·✓
✓
PEW-Related Same/es
PEW-1
PEW-3
PEW-4 ________ ~-
B-34
F-55
G-50
G-88
H-59
H-79
1st Quarter
voe
(82608)
✓
✓
(Full TCLP)11
(Full TCLP) 11
✓
✓
✓
✓
✓
✓
✓
✓
✓
✓
✓
✓
✓
voe
(82608)
✓
✓
✓
✓
-
Eth. Glycol
(GC/FJD)
✓
✓
svoc
(8270C}
✓
✓
✓
✓
--------
Table 1. 2000 Sampling Matrix-CNA Holdings, lne.-Shelby, NC
TDC
(9060)
✓
✓
✓
✓
2nd Quarter
voe
(8260B)
✓
✓
Eth. Glycol
(GC/FlDJ
---------
TDC
(9060}
3rd Quarter
voe
(82608)
Eth. Glycol
(GC/FID}
TDC
(9060)
(Ql . .b!!DP.!!}9 Discontinued on ~.@1/98) ___ ~-____ _
✓
✓ ✓
✓
✓
✓ ✓
✓
✓
✓
✓
✓
✓
✓
✓
voe
(8260B)
✓
✓
✓
✓
svoc
(8270C)
-
4th Quarter
voe
(82608)
-
Eth. Glycol
(GC/FID)
. . ---------------
-
Notes: 1/ TCLP Analyses as specified in Attachment 2 of most current, approved Sampling & Analysis Plan (KF&A, April 1998)
CNA lloldings, lnc.--Shclby, NC
OU-I Semiannual Report (July '00-Dec '00)
-
== liiil
~
IT-1
IT-2
IT-3 ...
IT-4
IT-5
IT-6
IT-7
IT-SR
IT-9
* ADF:
iiiil ----
July 2000 August 2000
Total Total
Gallons ADP Gallons ADF*
1,304 42 1,130 36
787 25 771 25
1 451 47 1,811 58
1,556 50 1,608 52
6,087 196 6,213 200
1 358 44 757 24
2,188 ·71 1,336 43
14,382 464 11,010 355
12 533 404 10 807 349
41,646 35,443
----

-
Table 2. Inner Tier Production Data
July '00 --Dec. '00
CNA Holdings, lnc.-Shelby, NC
September 2000 October 2000
Total Total
Gallons ADP Gallons ADP
1,257 42 957 31
688 23 1,731 56
1 941 65 1 918 62
2,358 79 2,774 89
5,317 177 6,720 217
1 121 37 2 216 71
2,213 74 3,256 105
11,405 380 12,640 408
13 768 459 10,089 325
40,068 42,301
Average Daily Flow based on CNA production records (Attachment 1),
Calculated as total flow divided by the number of days in the month.
--
November 2000
Total
Gallons ADF*
885 30
465 1 6
1 678 56
2,694 90
5,945 198
.J. 002 ... 33
2,783 93
12,214 407
12 204 407
39,870
----
December 2000 July-Dec. '00
Total
Gallons ADP Total Gallons
1,179 38 6,712
511 16 4,953
1,636 53 10 435
2,764 89 13,754
6,633 214 36,915
3 0 6,.45_7_
2,890 93 14,666
9,911 320 71,562
11 583 374 70 984
37,110 236,438
CNA Holdings, /nc.-Shclby, NC
OU·/ Semiannual Report (July '00 • Dec. '00)
-
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Table 3. Inner Tier TOC Data
July '00 --Dec. '00
CNA Holdings, lnc.-Shelby, North Carolina
(all results reported in ppm)
Influent Effluent % Reduction
Date
7 /6/00 1570 14 99.1
7/12/00 1350 10 99.3
7/18/00 1690 6 99.6
7/26/00 1360 14 99.0
........... 8/3/00. 2500 12 99.5 ······················ .. -·-················•········································································
8/8/00 2270 16 99.3
8/16/00 1790 19 98.9
8/24/00 1510 16 98.9
........ 8/3 0100 .................... 1. 800 ............................... 1.o .................................. 99 .4 .......... ..
9/7 /00
9/12/00
9/20/00
1360
1350
1310
19
14
1 5
98.6
99.0
98.9
9/26/00 2520 15 99.4
......... 1.0/ 4/00 ..................... 2220 .............................. 1,7 ............................... !l.!l.:.?. .......... ..
10/11/00
10/19/00
10/25/00
2300
1320
1280
20
28
35
......... 1.1./.1/00 .................... 1, 440 .............................. 4 8 ..... ..
11 /8/00 1360 34
11/14/00 1640 33
11/22/00 NS11 NS11
99.1
97.9
97.3
96.7 ························· 97.5
98.0
11/29/00 NS 11 NS11
......................................................... 11 ................................... 11 .................................................. .
1 2/5/00 NS NS -
12/13/00 1500 64 95.7
12/20/00 1370 75 94.5
12/26/00 1410 30 97.9
Average: 1662
Notes: 1/ No sample, lost in transport
25 98.4
CNA Holdings, lnc.-Shelby, NC
OU-1 Semiannual Report (July '00 -Dec. '00)
-------------------
Table 4. Summary of Selected Water-Quality Constituents (3rd Quarter 2000)
(All results reported in milligrams per liter)
CC-33 K-28 V-23
Total Organic Carbon NA 11 16.7 11700
Ethylene glycol NA NA NA
Volatile Organics
Acetone <0.010 <0.010 0.47
Benzene <0.005 0.01 0.021
2-butanone (MEK) <0.010 <0.010 0.42
Carbon disulfide <0.005 <0.005 0.041
Chlorobenzene <0.005 <0.005 <0.005
Trichloroethene 0.0059 <0.005 <0.005
Notes: 1 / NA ; Sample not analyzed for indicated constituents
2/ J ; Estimated Concentration
HH-48
NA
NA
<0.010
<0.005
<0.010
<0.005
<0.005
0.072
Inner Tier Inner Tier
HH-77 Influent Effluent
NA 1580 1 2
NA 802J21 <7.0
<0.010 0.13 <0.010
<0.005 0.029 <0.005
<0.010 <0.010 <0.01 0
<0.005 0.052 <0.005
<0.005 0.02 <0.005
0.14 <0.005 <0.005
CNA Holdings, /nc.-Shelby, NC
OU-/ Semiannual Report (July '00 -Dec. '00)
-------------------
Table s. Summary of Selected Water-Quality Constituents (4th Quarter 2000)
(All results reported in milligrams per liter)
K-28 V-23
Total Organic Carbon 1 63J ,, 10800
Ethylene glycol NA 21 NA
Volatile Organics
Benzene NA NA
Chlorobenzene NA NA
Notes: 1/ J = Estimated Concentration
2/ NA = Sample not analyzed for indicated constituent(s)
Inner Tier
Influent
1020
779
0.013
0.013
Inner Tier
Effluent
25.9
<7.0
<0.005
<0.005
CNA Holdings, lnc.--Shelby, NC
OU-1 Semiannual Report (July '00 -Dec. '00)
-------------------
Table 6. Summary of Selected PEW-Related Water Quality Constituents (3rd Quarter 2000)
(All results reported in milligrams per liter)
F-55
Semivolatile Organics
1, 1 biphenyl 101
Biphenyl ether 292
dibenzofuran 0.34
naphthalene 0.71
phenol 0.058
4-methylphenol (p-cresol) 0. 11
Volatile Organics
Acetone 0.021
Benzene 0.054
cis-1,2-dichloroethene <0.005
Trichloroethene <0.005
2 Butanone (M EK) 0.015
PEW-1 PEW-3
<0.010 <0.010
<0.010 <0.010
<0.010 <0.010
<0.010 <0.010
<0.010 <0.010
<0.010 <0.010
<0.010 <0.010
<0.005 <0.005
<0.005 <0.005
0.0071 <0.005
<0.005 <0.005
PEW-4
0.012
0.041
<0.010
<0.010
<0.010
<0.01 0
<0.010
<0.005
0.008
0.053
<0.005
CNA Holdings, lnc.-Shelby, NC
OU-1 Semiannual Report (July '00 -Dec. '00)
----
0
0
0
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.......,_l..,..T,..f,--
Atn!PEWE..---....,. __ _
-----
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-

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1-1-59 0 ,'
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0 400
-----
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Kubal-Furr & Associates
-Envinmmental Consultants -
Figure I-Site Location
Ce/an= North Am~. Inc.
Shd/,y. Nart h Carolina
-
----
D
D
Legend
0
A ·-♦ -<) o..wno,E.-.--:a + -T'"'E .. __ ~
♦---c-s--•
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.....,_f'EWE,.__ ~---
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---
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-----
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' '
----
Inner Tier Extraction wnn Water-levels
' 1--
' '
IT-1 = 782.11
IT-2 = <783.46
IT-3 = <778.56
IT-4 = 776.29
IT-5 = 779.14
IT-6 = <777.10
IT-7 : <790.57
IT-SR = 787.54
IT-9 = Nol Measured
Kubal-Furr & Associates
-Envimnmcntal Consultants -
f/qure 2-Potentiometric Surface Map
Shallow Saprofiu----Jufy !8, 2000
Celanei,,:, Nortl, J\meric;a. Inc.
Shelby, Nort/1 Carolina
- -- -
0
Q
leg~nd
• ~ 0
_..__.,._
A --~-♦ 1)o..,T,..E4act,oo,-• + _T..,E.nmon-* ♦ f'!;WE,__,\'\loll •
-o.-,-~---·-~-___ E4" __ ----C ---... -,,..,,,=-~=
□---
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0 400
-
' ' ' ' .& PZ-10
747_411\
"""'' 51.91
' '
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--
c:, r
Kubal-Furr & Associates
-Environmental Consultants -
flgun: 3-Potent.iomeuic Surf.ace M.ap
Oup SaprolitdUp~r Bcdrocl:-
Ju/y 18, 2000
~NorUl,',t"""""'·'""· 5,..,1,y,NcnJtC.rvlil ...
-
- -------- -
850.00 A -i~-=-=-=-=-=-=-=-=-=-=-=--=~P~l~•:o~t ~N~•=•--=========1!:::::::=------------w.astewater Treatment Area ------------•
830.00
0-27
824.92
D-35 810.00 · 824.60
G-50
812.48 J-28
802.59
790.00 D-56
824.60
770.00
750.00
730.00
710.00
690.00
Legend
/ line of equal fluid potential (ft msl) = Bedrock -610 (d.lshed where inlened) Horizont.rl $;.it!" in Fc"t
Potenliometric Surface c::::J Saprolite 0 400 800 •
•
Screened Interval of Well -Inferred direction of ground-water
movement
• C ::,
~ " • a. e a. '
- --
A' 85000
830.00
810.00
790.00
77000
750.00
730.00
710.00
69000
Kubal-Furr & Associates
-Environmental Consultants -
Figure 4-Hydrv!J&alc!Jic cn:,5-!>-SXt:km
A·A'-July 18, 2000
Ce!.an,-:~ North /lm"rica, Jn.:;.
Shdby. Nortli Carolina
----
A-39 e .,,,,
Legend
... _
¢-o.i.,-~-· +-n•E ... __
-+-PEWE..--Q __ _
✓;,,,,/=-~=
□-
0 ---L>. --♦ .-o...._E ___
• _.,,no.,r-E"'od»O-
" _,.P(WE--. ----···~ 0 "'°
----- ---
(
- ---
Inner Tier Extraction Well Water-I avels
IT-1 = Not Measured
IT-2 = Nol Measured
IT-3 = Not Measured
IT-4 = 776.18
IT-5 = 775.94
IT-6 = <776.80
IT-7 = <785.95
IT-8R : 788.73
IT-9 = Not Measured
Kubal-Furr & Associates
-Environmental Consultants -
F~un: 5-T'otentiometri,:; Surface Map
Slianow Saprotite---Octot>er 24, 2000
Ce!ane,;,e North t\merica, Inc.
SIie/by, North Carolina
--

-
-
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♦ ❖ O.,o,Tlo,f,1,-w.1 • + -n•E.., __ "9° ... -£--■ .··.· •
........ -eu., --....... o..i.,T ... l'otr0<110nl'M
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---

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----
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OH _!..-45-~pz.11
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760.38
-~ '
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Kubal-Furr & Associates
-Environmental Consultants -
Fiqurtt 6-Pot.cnt.iomet,ric Surface Map
Deep Saprolite/Upper Be.drocl-Gaot>er 24, 2CXJO
~NorlnN,.,,..,,,,Jr,,: .
Shotby. North C..r,,in.o
-
-- --- ----- - - -
85000 A -.i.'.~-=-=-=-=-=-=-=-=-=-=-=-=-:~l~a~nl~A~r•~•'..:::========~~::::::~----------~wastewater Treatment Area ------------
830.00
810.00
790.00
770.00
750.00
730.00
710.00
690.00
,I --810
•
D--27-
823.55
D-35
823.24
D-56
823.26
line of equal fluid potential (ft msl)
(dashed..tie<emfen'ed)
Potentiometric Surface
Inferred direction of ground-water
movement
=
CJ
l I
Bedrock
Saprolite
G-50
811.79
Screened Interval of Well
Horizont;t/ Scali, iri Feet
0 400 800
- - ---
A' 85000
830.00
810.00
790.00
77000
750.00
730.00
710.00
690.00
Kubal-Furr & Associates
-Environmental Consultants -
FiguM 7-Hydrogco/ogic; Cro:;;:;;·S~t.ion
A-A'---October 24, 2000
Cdane!i<I' North Am1:rica. Im:.
SM/by. North Carolina
-
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I Attachment 1
I Operation and Maintenance Data
July-December, 2000
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Kubal-Furr & Associates
I
I INNER TIER
DAILY FLOW
I JULY.
2000 IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9
I 07/01/00 66 26 48 0 192 46 88 990 491
07/02/00 68 25 50 0 199 67 97 996 505
07/03/00 67 27 49 0 221 67 92 977 494
I 07/04/00 66 26 48 0 213 66 93 642 489
07/05100 70 26 49 55 212 69 94 1208 518
07/06/00 57 26 48 60 203 66 91 277 397
I 07107/00 61 26 49 64 218 52 86 353 425
07/08/00 16 27 47 61 199 60 71 342 426
07/09/00 22 27 48 60 203 63 77 367 433
07/10/00 14 26 47 63 198 47 89 376 438
I 07/11/00 16 23 49 64 196 53 97 376 438
07/12/00 1 0 46 52 178 35 82 331 398
07/13/00 40 39 49 57 203 39 96 388 483
07/14/00 57 30 45 52 194 41 76 366 458
I 07/15/00 49 31 51 58 214 42 85 398 507
07/16/00 40 26 46 54 207 42 77 382 487
07/17/00 39 26 47 54 209 46 80 387 500
07/18/00 37 26 50 48 209 49 82 394 514
I 07/19/00 38 25 45 66 208 48 91 395 519
07/20/00 40 25 46 63 204 39 91 392 512
07/21/00 39 26 46 63 203 31 90 394 519
07/22/00 29 21 32 45 144 30 58 275 360
I 07/23/00 44 27 50 57 186 32 50 355
07/24/00 44 28 46 61 195 26 30 397 0
07/25/00 39 22 42 56 176 6 34 359
I 07/26/00 45 30 46 56 179 36 33 362 471
07/27/00 41 28 45 59 187 36 35 388 634
07/28/00 40 24 43 57 179 23 32 368 598
07/29/00 41 0 45 56 185 38 91 368 0
I 07/30/00 38 39 44 58 185 37 0 387 0
07/31/00 40 29 55 57 188 26 0 392 517
I AVG: 42 25 47 50 196 44 71 464 404
TOTAL: 1304 787 1451 1556 6087 1358 2188 14382 12533
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I 1
GROUNDWATER MONTHLY MONITORING:
RAINFALL DATA
JULY
DATE INCHES/DAY
07/01/00 0.00
07/02/00 0.00
07/03/00 0.00
07/04/00 0.00
07/05/00 0.00
07/06/00 0.60
07/07/00 0.00
07/08/00 0.00
07/09/00 0.00
07/10/00 o.oo
07/11/00 1.20
07/12/00 0.60
07/13/00 0.00
07/14/00 0.10
07/15/00 0.00
07/16/00 0.00
07/17/00 0.00
07/18/00 0.00
07/19/00 0.20
07/20/00 0.00
07/21/00 0.00
07/22/00 0.00
07/23/00 0.00
07/24/00 0.10
07/25/00 0.00
07/26/00 0.00
07/27/00 0.40
07/28/00 0.00
07/29/00 o.oo
07/30/00 0.00
07/31/00 0.20
TOTAL 3.40
2
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--- -- - ---- --Quarterly O&M Plan Checklist-HNA Holdings, lnc./Shelby, NC
Outer Tier Well
OT-2R
OT-3
OT-4
OT-5
OT-6
OT-SA
OT-7
OT-8
Ground-Water
Treatment Sys.
Open Sample
Port
X
X
X
X
X
X
X
X
Energize
AS Blower
Y-V-1008
Energize Verify De-energize Close Sample Verify Heater
Pump Discharge Pump Port Operation
X X X X X
X X X X X
X X X X X
X X X X X
X X X X X
X X X X X
X X X X X
X X X X X
Energize Energize Energize Energize
Transfer Pump Transfer Pump Transfer Pump Transfer Pump
Y-P-1007A Y-P-1007B Y-P-1008A Y-P-1008B
-- - - -- -
Form Completed by: TONY BRYANT
Date: 7/3/00
Secure Well
Vault Comments
X
X
X
X
X
X
X
X
Comments
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
ACTION
DATE WELL# PROBLEM DATE ACTION
7/5/00 #4 LOW FLOW 7/5/00 REPAIR AIR LINE
-·--•• , ,J '-" ......... , -·
7/6/00 #8 LOW FLOW 7/6/00 METER
7/13/00 #1 VERY LOW FLOW 7/13/00 NEW BLADDER, EXHUSTER &RESET PUMP
7/13/00 #2 NO FLOW 7/13/00 RESET PUMP
7/22/00 CARBON FILTER 7/22/00 AIR LANCED
7/23/00 I.T. LINE LEAK 7/23/00 REPLACED WATER LINE
7/31/00 #9 NO FLOW 7/31/00 RESET PUMP
4
MECHANIC
P.P.
P.P.
P.P.
P.P.
pp
P.P.
P.P.
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·1
DAILY REFERENCE SHEET:
I DATE: IT. EQ. PLT. DEC. DEC. WAS MIX MIX MIX NIT PHOS MIX F/M
JULY. INF. TNK. SEP. LIQ LIQ LIQ ADD ADD LIQ WAS 5/DAY
2000 COD. COD. COD. COD, TSS. TSS MLSS !ill PHOS GALS LBS gr. GALS ELM AVG.
I 1 5300 4770 4780 210 130 1556 110 24.0 0 200 0 0.27
2 4740 4080 1892 121 21.6 1 1 180 0 0.00
3 5940 4400 4350 203 224 6830 1512 116 35.0 0 0 190 135 0.26
4 6010 3860 3540 181 110 9240 2060 146 24.7 0 0 160 135 0.15
I 5 5170 3830 8320 1528 98 16.8 1 2 150 135 0.00 0.14
6 4260 4600 4150 174 30 6800 1496 119 50.2 0 0 150 135 0.25 0.13
7 5930 5150 7750 1544 98 39.0 0 0 150 135 0.00 0.13
8 4820 5060 4340 202 80 8070 1532 114 43.5 0 0 160 135 0.25 0.13
9 3870 4740 6340 1556 86 27.5 1 0 160 135 0.00 0.10
I 10 4170 3490 4320 205 110 6240 1504 110 30.5 0 0 160 135 0.26 0.15
11 4500 4250 6010 1372 112 16.6 0 2 150 135 0.00 0.10
12 4220 3450 3840 254 510 7090 1316 100 35.5 0 0 150 135 0.26 0.15
13 3130 4030 8320 1228 75 22.5 1 150 135 0.00 0.10
I 14 4450 3460 3570 220 100 8460 1532 85 29.0 0 150 135 0.21 0.14
15 4850 4020 3360 253 710 8620 1804 120 13.6 1 200 135 0.17 0. 13
16 3990 2970 2012 109 30.0 0 0 250 0 0,00 0.13
17 4740 4430 4330 265 540 6730 1500 93 36.0 0 0 200 135 0.26 0.13
18 4990 4150 3160 250 260 7320 2268 98 38.0 0 0 200 135 0.12 0.15
I 19 3970 3490 6780 1460 85 35.8 1 0 160 135 0.00 0.11
20 4560 3590 2870 243 120 7060 1456 100 31.4 0 0 120 135 0.18 0.11
21 4060 3640 3730 271 200 7040 1576 85 23.8 1 120 135 0.21 0.15
22 4410 2840 7380 1268 95 23.2 1 120 135 0.00 0.10
I 23 4530 3010 3430 275 220 4000 1260 160 35.5 0 0 120 135 0.24 0.13
24 6620 4670 4400 1492 106 25.2 0 0 100 135 0.00 0.13
25 6090 4420 6820 1416 107 29.5 0 0 100 135 0.00 0.09
26 6180 4840 4780 263 20 7920 1044 106 30.2 0 0 100 135 0.41 0.13
27 4070 4280 8200 1736 80 20.2 1 100 135 0.00 0.13
I 28 3630 3780 4010 262 180 11180 1106 116 35.4 0 0 100 135 0.32 0.15
29 4180 4020 1288 100 17.6 1 110 0 0.00 0.15
30 7000 4400 3940 250 160 8000 996 115 25.5 0 0 70 135 0.35 0.22
31 4420 4210 9040 1212 95 17.5 1 2 70 135 0.00 0.13
I AVG: 4800 4062 3694 221 206 7141 1501 105.2 28.5 0 0 145 118 0.13
MAX: 7000 5150 4780 275 710 11180 2268 160.0 50.2 1 2 250 135 0.41
MIN: 3130 2840 0 0 0 0 996 75.0 13.6 0 0 70 0 0.00
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INNER TIER COMBINED INFLUENT #2 ITCI I
PAGE N0.1
JULY.2000 I DATE: FLOW: PH: COD: TSS: TOG:
GPO pH ppm ppm ppm
07/01/00 1947 5.6 5300 45 I 07/02/00 2007 5.3 4740 10
07/03/00 1994 5.6 5940 20
07/04/00 1643 5.4 6010 9 I 07/05/00 2301 5.3 5170 10
07106100 1225 5.3 4260 34 1570
07107/00 1334 5.3 5930 11 I 07/08/00 1249 5.3 4820 14
07109100 1300 5.3 3870 3
07/10/00 1298 5.4 4170 8 I 07/11/00 1312 5.3 4500 10
07/12/00 1123 5.3 4220 4 1350
07/13/00 1394 5.5 3130 6
07/14/00 1319 5.2 4450 10 I 07/15/00 1435 5.3 4580 6
07/16/00 1361 5.3 3990 8
07/17/00 1388 5.3 4740 3 I 07/18/00 1409 5.3 4990 3 1690
07/19/00 1435 5.3 3970 11
07/20/00 1412 5.2 4560 5
07/21/00 1411 5.2 4060 7 I 07/22/00 994 5.2 4410 1
07/23/00 802 5.3 4530 20
07/24/00 · 827 5.2 6620 10 I 07/25/00 735 5.1 6090 10
07/26/00 1258 5.2 6180 14 1360
07/27/00 1453 5.2 4070 6 I 07/28/00 1364 5.2 3630 7
07/29/00 824 5.2 4180 4
07/30/00 788 5.2 7000 11
07/31/00 1304 5.1 4420 21 I
AVG: 1343 5.3 4791 11 1493
MAX: 2301 5.6 7000 45 1690 I MIN: 735 5.1 3130 1350
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I GROUNDWATER MONTHLY MONITORING:
INNER TIER EQUALIZATION TANK: ITEQT
PAGE NO. 2
I JULY.2000
DATE: PH: COD: OT WATER ADDED
pH ppm gal
I 07/01/00 7.3 4770 300
07/02/00 7.5 4080
07/03/00 7.2 4400
I 07/04/00 7.3 3860
07/05/00 7.3 3830
07/06/00 7.5 4600
I 07107/00 7.4 5150
07/08/00 7.3 5060
07/09/00 7.4 4740
I 07/10/00 7.5 3490
07/11/00 7.5 4250
07/12/00 7.5 3450
07/13/00 7.7 4030
I 07/14/00 7.3 3460
07/15/00 7.6 4020 400
07/16/00 7.6 2970
I 07/17/00 7.6 4430
07/18/00 7.5 4150
07/19/00 7.6 3490
I 07/20/00 7.6 3490
07/21/00 7.6 3640 560
07/22/00 7.7 2840
07/23/00 7.7 3010
I 07/24/00 7.6 4670
07/25/00 7.6 4420
07/26/00 7.6 4840
I 07/27/00 7.6 4280
07/28/00 7.7 3780
07/29/00 8.1 4020
07/30/00 7.7 4400
I 07/31/00 7.8 4210
AVG: 7.5 4059 420
I MAX: 8.1 5150 560
MIN: 7.2 2840 300
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I 7
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GROUNDWATER MONTHLY MONITORING: I AFTER PLATE SEPARATOR BEFORE SBR: SBRI
PAGE NO. 3
JULY.2000 I DATE: PH: COD: TSS:
pH ppm ppm
07/01/00 5.9 4780 8 I
07/02/00
07/03/00 6.9 4350 112 I 07/04/00 5.9 3540 80
07105100
07/06/00 6.9 4150 56
07107/00 I 07/08/00 5.9 4340 20
07/09/00
07/10/00 5.9 4320 24 I 07/11/00
07/12/00 5.9 3840 52
07/13/00
07/14/00 6.1 3570 20 I 07/15/00 7.2 3360 64
07/16/00
07/17/00 7.3 4330 76 I 07/18/00 7.5 3160 52
07/19/00
07/20/00 6.1 2870 16 I 07/21/00 6.0 3730 32
07/22/00
07/23/00 5.8 3430 88
07/24/00 I 07/25/00
07/26/00 7.6 4780 92
07/27/00 I 07/28/00 7.7 4010 80
07/29/00
07/30/00 5.8 3940 36
07/31/00 I
AVG: 6.5 3912 53
MAX: 7.7 4780 112 I MIN: 5.8 2870 8
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I GROUNDWATER MONTHLY MONITORING:
SBR MIXED LIQUOR: SBRML
I PAGE NO.4
JULY.2000 SETT. SLUDGE 5/DAY
DATE: PH: NH3N: PO4: DO: MLSS: MLVSS: SOLIDS: WASTED F/M: F/M:
pH ppm ppm ppm ppm ppm ml/I gal ratio ratio
I 07/01/00 8.8 110 24.0 5.7 1556 200 0 0.27
07/02/00 8.4 121 21.6 5.3 1892 180 0 0.00
I 07/03/00 9.0 116 35.0 6.4 1512 190 135 0.26
07/04/00 8.8 146 24.7 6.7 2060 160 135 0.15
07/05/00 8.8 98 16.8 5.7 1528 1092 150 135 0.00 0.14
07/06/00 8.8 119 50.2 5.6 1496 150 135 0.25 0.13
I 07107/00 8.7 98 39.0 3.7 1544 150 135 0.00 0.13
07/08/00 8.9 114 43.5 6.6 1532 160 135 0.25 0.13
07/09/00 8.7 86 27.5 5.5 1556 160 135 0.00 0.10
I 07/10/00 8.9 110 30.5 5.4 1504 160 135 0.26 0.15
07/11/00 8.3 112 16.6 4.4 1372 1165 150 135 0.00 0.10
07/12/00 8.9 100 35.5 5.7 1316 150 135 0.26 0.15
I 07/13/00 8.9 75 22.5 1.0 1228 150 135 0.00 0.10
07/14/00 8.8 85 29.0 5.7 1532 150 135 0.21 0.14
07/15/00 8.8 120 13.6 5.5 1804 200 135 0.17 0.13
07/16/00 8.6 109 30.0 0.0 2012 250 0 0.00 0.13
I 07/17/00 8.8 93 36.0 3.4 1500 200 135 0.26 0.13
07/18/00 8.7 98 38.0 4.8 2268 1216 200 135 0.12 0.15
07/19/00 8.7 85 35.8 2.0 1460 160 135 0.00 0.11
I 07/20100 8.9 100 31.4 5.7 1456 120 135 0.18 0.11
07/21/00 8.8 85 23.8 4.9 1576 120 135 0.21 0.15
07/22/00 8.8 95 23.2 4.6 1268 120 135 0.00 0.10
07/23/00 8.9 160 35.5 4.9 1260 120 135 0.24 0.13
I 07/24/00 8.8 106 25.2 5.0 1492 100 135 0.00 0.13
07/25/00 8.9 107 29.5 5.9 1416 896 100 135 0.00 0.09
07/26/00 8.9 106 30.2 6.6 1044 100 135 0.41 0.13
I 07127/00 8.8 80 20.2 5.7 1736 100 135 0.00 0.13
07/28/00 8.9 116 35.4 6.7 1106 100 135 0.32 0.15
07/29/00 8.8 100 17.6 5.6 1288 110 0 0.00 0.15
07/30/00 8.9 115 25.5 5.9 996 70 135 0.35 0.22
I 07/31/00 8.9 95 17.5 4.4 1212 860 70 135
AVG: 8.8 105 29 5 1501 1046 145 118 0.14 0.13
I MAX: 9.0 160 50 7 2268 1216 250 135 0.41 0.22
MIN: 8.3 75 14 0 996 860 70 0 0.00 0.09
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I 9
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GROUNDWATER MONTHLY MONITORING: I SBR EFFLUENT:(DECANT) #4 SBRE
PAGE NO. 5
JULY.2000 WAS. NH3N PHOS. I DATE: FLOW: COD: TSS: TSS ADDED: ADDED:
GPO ppm ppm ppm gal lbs
07/01/00 2550 210 130.0 0 I 07/02/00 0 1 1
07/03/00 1964 203 224 6830 0 0
07/04/00 2379 181 110.0 9240 0 0 I 07/05/00 0 8320 1 2
07/06/00 1875 174 30.0 6800 0 0
07/07/00 0 7750 0 0 I 07/08/00 2295 202 80 8070 0 0
07/09/00 0 6340 1 0
07/10/00 2130 205 110 6240 0 0
07/11/00 0 6010 0 2 I 07/12/00 2105 254 510 7090 0 0
07/13/00 0 8320
07/14/00 2339 220 100 8460 0 I 07/15/00 2356 253 710 8620 1
07/16/00 0 0 0
07/17/00 1890 265 540 6730 0 0 I 07/18/00 2100 250 260 7320 0 0
07/19/00 0 6780 0
07/20/00 1953 243 120 7060 0 0
07/21/00 1950 271 200 7040 I 07/22/00 0 7380 1 1
07/23/00 2025 275 220 4000 0 0
07/24/00 0 4400 0 0 I 07/25/00 0 6820 0 0
07/26/00 2163 263 20 7920 0 0
07/27/00 0 8200 1 1
07/28/00 1763 262 80 11180 0 0 I 07129100 0 1 1
07/30/00 1875 250 160.0 8000 0 0
07/31/00 0 9040 2 I
AVG: 1152 234 212 7406 0 0
MAX: 2550 275 710 11180 2
MIN: 0 174 20 4000 0 0 I • DID NOT PROCESS SBR .
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I GROUNDWATER MONTHLY MONITORIN(
INNER TIER CARBON FILTER EFFLUENT #8 ITEF
PAGE NO. 7
I JULY.2000
DATE: PH: COD: TOG: TSS:
pH ppm ppm ppm
I 07/01/00
07102100
07/03/00
I 07/04/00
07/05/00
07/06/00 8.6 141 14 10
I 07107/00
07/08/00
07/09/00
I 07/10/00
07/11/00
07/12/00 8.1 169 10
07/13/00
I 07/14/00
07/15/00
07/16/00
I 07117100
07118100 8.0 200 6
07/19/00
07/20100
I 07/21100
07122100
07/23/00
I 07/24/00
07/25/00
07/26/00 8.3 107 14
I 07/27/00
07/28/00
07/29/00
07/30/00
I 07/31/00
AVG: 8.3 154 11 10
I MAX: 8.6 200 14 10
MIN: 8.0 107 6 10
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I 11
I
INNER TIER
DAILY FLOW I
AUG. I
ZQ9Q lI:1 IT-2 IT-3 ~ IT-5 IT-6 IT-7 1H 1H
08/01/00 39 29 33 59 184 10 10 390 254 I 08/02/00 39 25 44 60 184 25 10 388 0
08/03/00 39 27 44 58 176 26 13 390 43
08/04/00 39 21 46 61 201 17 15 402 74 I 08/05/00 40 25 44 60 182 26 18 392 0
08/06/00 38 25 42 61 163 32 0 384 0
08/07/00 40 26 47 61 171 29 18 397 445
08/08/00 41 24 48 62 174 25 0 390 120 I 08/09/00 41 25 58 60 191 29 0 392 360
08/10/00 41 26 70 61 194 31 0 390 565
08/11/00 40 26 69 61 207 18 0 389 562
08/12/00 38 25 69 60 222 22 0 387 559 I 08/13/00 37 25 67 60 218 24 0 380 293
08114100 37 25 69 60 222 28 0 389 3
08115/00 39 26 68 62 218 29 18 384 513
08116100 39 26 66 50 226 32 43 378 564 I 08117100 38 24 65 103 216 29 74 379 421
08/18/00 40 23 68 112 216 27 91 405 485
08119100 37 22 64 108 205 28 82 355 275
08120100 36 24 62 79 181 21 78 330 239 I 08/21/00 34 26 63 55 192 20 81 340 59
08122/00 34 25 62 51 212 25 81 345 166
08123100 33 27 60 8 209 22 83 342 438 I 08124100 33 23 60 0 373 20 78 325 541
08/25100 33 25 61 0 27 26 81 300 542
08126100 32 25 63 0 200 27 79 242 540
08127100 30 24 60 0 181 23 77 243 543 I 08128100 31 24 59 12 209 24 81 260 528
08129100 32 24 61 0 231 21 76 292 583
08130100 30 26 60 52 241 15 75 297 549
08131100 30 23 59 72 187 26 74 333 543 I
AVG: 36 25 58 52 200 24 43 355 349
TOTAL: 1130 771 1811 1608 6213 757 1336 11010 10807 I
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GROUNDWATER MONTHLY MONITORING:
RAINFALL DATA
AUGUST 2000
DATE INCHES/DAY
08/01/00 0.20
08/02/00 0.00
08/03/00 0.30
08/04/00 0.05
08/05/00 0.00
08/06/00 0.00
08/07/00 0.00
08/08/00 0.00
08/09/00 0.20
08/10/00 0.00
08/11/00 0.00
08/12/00 0.00
08/13/00 0.00
08/14/00 0.00
08/15/00 0.00
08/16/00 0.00
08/17/00 0.00
08/18/00 0.00
08/19/00 0.00
08/20/00 0.00
08/21/00 0.00
08/22/00 0.00
08/23/00 0.00
08/24/00 0.00
08/25/00 1.10
08/26/00 0.00
08/27/00 0.00
08/28/00 0.00
08/29/00 0.00
08/30/00 0.10
08/3li00 0.00
TOTAL 1. 95
13
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
ACTION
DATE WELL# PROBLEM DATE ACTION
8/14/00 #9 LOW FLOW 8/14/00 CLEANED PROBE
8/16/00 #7 LOW FLOW 8/16/00 REPLACE EXHUASTER & BLADDER
8/28/00 #4 LOW FLOW 8/28100 ADJUST REGULATOR &AIRLINE FITTINGS
8130100 #4 LOW FLOW 8130/00 REPLACED AIR LINE
1 4
MECHANIC
P.P.
P.P.
P.P.
P.P.
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I DAILY REFERENCE SHEET:
I DATE: IT. EQ. PLT. DEC. DEC. WAS MIX MIX MIX NIT PHO$ MIX F/M
AUG. INF. TNK. SEP. LIQ LIQ LIQ ADD ADD LIQ WAS 5/DAY
Z2QQ COD. ~ COD. COD. liS. .Ifili ~ Jill etiOS MbS J,fil SET. ~ ELM AVG.
I 3080 4230 3460 228 120 6720 1166 165 35.4 0 0 70 135 0.26
2 6350 3440 7920 1248 105 20.2 1 2 70 135 0.00
3 8800 3860 4800 243 120 9180 1212 161 33.5 0 0 70 135 0.35
4 7180 5270 8300 1180 103 26.5 0 0 70 135 0.00
5 5690 4220 4350 268 950 2260 1052 140 43.9 0 0 60 100 0.37 0.20
I 6 7820 3960 1160 112 20.2 1 1 50 0 0.00 0.14
7 6650 5590 1068 129 65.0 0 0 70 0 0.00 0.14
8 3680 4630 4390 314 80 7760 1008 155 72.0 0 0 70 100 0.39 0.15
9 6370 4950 1056 109 55.0 0 0 70 0 0.00 0.15
I 10 3970 5240 5260 282 20 9180 1024 132 72.8 0 0 70 100 0.46 0.17
11 3730 3900 900 100 50.5 0 0 70 0 0.00 0.17
12 5860 3300 4230 274 120 7460 984 100 55.0 0 0 50 100 0.38 0.25
13 3570 3410 988 86 50.3 0 50 0 0.00 0.17
14 6890 3750 3280 294 200 6800 964 119 51.5 0 0 50 100 0.30 0.23
I 15 6020 3780 928 116 49.0 0 0 50 0 0.00 0.14
16 3800 3900 3990 403 320 7780 944 110 49.3 0 0 50 25 0.38 0.21
17 4000 3740 932 106 45.0 0 0 50 0 0.00 0.14
18 6420 3700 4250 365 320 9160 780 103 47.5 0 0 50 25 0.48 0.23
19 4750 4590 968 80 37.0 0 50 0 0.00 0.17
I 20 7290 4440 4520 413 240 6160 904 100 38.0 0 50 25 0.44 0.26
21 6270 4460 976 100 32.0 1 0 50 0 0.00 0.19
22 5910 3410 4120 418 360 8440 924 121 34.2 0 0 50 25 0.40 0.27
23 6050 4030 1020 101 25.2 0 0 50 0 0.00 0.17
I 24 3780 3870 4920 420 200 7560 968 126 30.5 0 0 50 25 0.45 0.26
25 4360 4370 900 88 20.3 1 50 0 0.00 0.17
26 4340 3620 3660 318 270 1700 920 106 25.2 0 0 50 25 0.35 0.24
27 4230 3780 928 85 18.0 1 1 50 0 0.00 0.16
28 4200 4300 3690 325 190 9000 1326 113 27.3 0 0 50 25 0.25 0.21
I 29 3350 3280 964 109 21.8 0 0 50 0 0.00 0.12
30 3880 4730 4410 330 170 7400 884 100 22.7 1 1 50 25 0.44 0.21
31 4030 3980 1000 133 23.8 0 0 50 0 0.00 0.14
I AVG: 5171 4120 3958 306 230 7575 1009 113.3 38.7 0 0 56 40 0.18
MAX: 7820 5590 5260 420 950 9180 1326 165.0 72.8 1 2 70 135 0.48
MIN: 3080 3280 0 0 0 2260 780 80.0 18.0 0 0 50 0 0.00
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2/16/01
15
I
INNER TIER COMBINED INFLUENT #2 ITC\ I
PAGE N0.1
AUGUST.2000 I DATE: FLOW: PH: COD: TSS: TOG:
GPO pH ppm ppm ppm
08/01/00 1008 5.2 3080 10 I 08/02/00 775 5.1 6350 9
08/03/00 816 5.0 6800 10 2500
08/04/00 876 5.2 7180 14 I 08105100 787 5.1 5690 13
08/06/00 745 5.1 7820 13
08/07/00 787 5.1 6650 2
08/08/00 884 5.2 3680 12 2270 I 08/09/00 1156 5.2 6370 19
08/10/00 1378 5.3 3970 8
08/11/00 1372 5.3 3730 6 I 08/12/00 1382 5.3 5860 7
08/13/00 1104 5.4 3570 9
08/14/00 833 5.2 6890 15 I 08/15/00 1357 5.2 6020 16
08/16/00 1424 5.3 3800 5 1790
08/17/00 1349 5.3 4000 11
08/18/00 1467 5.2 6420 12 I 08/19/00 1176 5.2 4750 7
08/20/00 1050 5.1 7290 10
08/21/00 870 5.1 6270 10 I 08/22/00 1001 5.2 5910 10
08/23/00 1222 5.1 6050 1
08/24/00 1453 5.3 3780 10 1510
08/25/00 1095 5.3 4360 7 I 08/26/00 1208 5.3 4340 19
08/27/00 1181 5.3 4230 3
08/28/00 1228 5.2 4200 25 I 08/29/00 1320 5.2 3350 11
08/30/00 1345 5.2 3860 12 1800
08/31/00 1347 5.3 4030 10 I AVG: 1129 5.2 5171 11 1974
MAX: 1467 5.4 7820 25 2500
MIN: 745 5.0 3080 1510 I
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16 I
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I GROUNDWATER MONTHLY MONITORING:
INNER TIER EQUALIZATION TANK: ITEQT
PAGE NO. 2
I AUGUST.2000
DATE: PH: COD: OT WATER ADDED
pH ppm gal
I 08/01/00 8.0 4230
08/02/00 12.4 3440
08/03/00 12.2 3860 300
I 08/04/00 11.8 5270
08/05/00 9.4 4220 400
08/06/00 7.7 3960
I 08/07/00 7.8 5590
08/08/00 7.7 4630
08/09/00 7.7 4950
08/10/00 7.2 5240 75
I 08/11/00 7.7 3900
08/12/00 7.3 3300
08/13/00 7.7 3410
I 08/14/00 7.6 3750
08/15/00 7.7 3780
08/16/00 7.6 3900 113
I 08/17/00 7.7 3740
08/18/00 7.6 3700
08/19/00 7.7 4590
08/20/00 7.7 4440
I 08/21/00 7.6 4460
08/22/00 7.7 3410 75
08/23/00 7.7 4030
I 08/24/00 7.7 3870 150
08/25/00 7.8 4370
08/26/00 7.7 3620
08/27/00 7.7 3780
I 08/28/00 7.6 4300
08/29/00 7.5 3280
08/30/00 7.7 4730
I 08/31/00
AVG: 8.2 4125 186
I MAX: 12.4 5590 400
MIN: 7.2 3280 75
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I 1 7
I
GROUNDWATER MONTHLY MONITORING: I AFTER PLATE SEPARATOR BEFORE SBR: SBRI
PAGE NO. 3
AUGUST.2000 I DATE: PH: COD: TSS:
pH ppm ppm
08/01/00 5.7 3460 20 I 08/02/00
08/03/00 10.6 4800 68
08/04/00 I 08/05/00 12.2 4350 52
08/06/00
08/07/00 I 08/08/00 8.4 4390 44
08/09/00
08/10/00 7.4 5260 64
08/11/00 I 08/12/00 6.9 4230 24
08/13/00
08/14/00 6.4 3280 16 I 08/15/00
08/16/00 6.4 3990 24
08/17/00
08/18/00 7.0 4250 64 I 08/19/00
08/20/00 7.0 4520 20
08/21/00 I 08/22/00 5.9 4120 40
08/23/00
08/24/00 6.0 4920 16
08/25/00 I 08/26/00 6.2 3660 40
08/27/00
08/28/00 6.7 3690 44 I 08/29/00
08/30/00 6.7 4410 32
08/31/00 I AVG: 7.3 4222 38
MAX: 12.2 5260 68
MIN: 5.7 3280 16 I
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18 I
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I GROUNDWATER MONTHLY MONITORING:
SBR MIXED LIQUOR: SBRML
PAGE NO. 4
I AUGUST.2000 SETT. SLUDGE 5/DAY
DATE: PH: NH3N: PO4: DO: MLSS: MLVSS: SOLIDS: WASTED F/M: F/M:
pH ppm ppm ppm ppm ppm ml/I gal ratio ratio
I 08/01/00 8.9 165 35.4 5.1 1166 70 135 0.26
08/02/00 8.7 105 20.2 2.3 1248 70 135 0.00
08/03/00 8.5 161 33.5 2.4 1212 70 135 0.35
I 08/04/00 8.7 103 26.5 1.1 1180 70 135 0.00
08/05/00 8.6 140 43.9 2.4 1052 60 100 0.37 0.20
08/06/00 8.5 112 20.2 2.1 1160 50 0 0.00 0.14
I 08/07/00 8.5 129 65.0 2.4 1068 70 0 0.00 0.14
08/08/00 8.5 155 72.0 2.1 1008 666 70 100 0.39 0.15
08/09/00 8.4 109 55.0 2.3 1056 70 0 0.00 0.15
08/10/00 8.4 132 72.8 2.4 1024 70 100 0.46 0.17
I 08/11/00 8.4 100 50.5 2.5 900 70 0 0.00 0.17
08/12100 8.5 100 55.0 2.5 984 50 100 0.38 0.25
08/13/00 8.5 86 50.3 1.9 988 50 0 0.00 0.17
I 08/14/00 8.5 119 51.5 1.9 964 50 100 0.30 0.23
08/15/00 8.4 116 49.0 1.8 928 620 50 0 0.00 0.14
08/16/00 8.4 110 49.3 3.3 944 50 25 0.38 0.21
I 08/17/00 8.4 106 45.0 2.4 932 50 0 0.00 0.14
08/18/00 8.4 103 47.5 2.5 780 50 25 0.48 0.23
08/19/00 8.3 80 37.0 2.2 968 50 0 0.00 0.17
08/20/00 8.4 100 38.0 2.6 904 50 25 0.44 0.26
I 08/21/00 8.4 95 32.0 0.8 976 50 0 0.00 0.19
08/22/00 8.5 121 34.2 1.8 924 608 50 25 0.40 0.27
08/23/00 8.5 101 25.2 2.3 1020 50 0 0.00 0.17
I 08/24/00 8.5 126 30.5 2.8 968 50 25 0.45 0.26
08/25/00 8.5 88 20.3 3.2 900 50 0 0.00 0.17
08/26/00 8.6 106 25.2 3.6 920 50 25 0.35 0.24
08/27/00 8.5 85 18.0 2.3 928 50 0 0.00 0.16
I 08/28/00 8.4 113 27.3 3.4 1326 50 25 0.25 0.21
08/29/00 8.4 109 21.8 2.4 964 680 50 0 0.00 0.12
08/30/00 8.4 100 22.7 2.2 884 50 25 0.44 0.21
I 08/31/00 8.5 133 23.8 2.5 1000 50 0 0.00 0.14
AVG: 8.5 113 39 2 1009 644 56 40 0.18 0.19
MAX: 8.9 165 73 5 1326 680 70 135 0.48 0.27
I MIN: 8.3 80 18 780 608 50 0 0.00 0.12
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I 19
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GROUNDWATER MONTHLY MONITORING: I SBR EFFLUENT:(DECANT) #4 SBRE
PAGE NO. 5
AUGUST.2000 WAS. NH3N PHOS. I DATE: FLOW: COD: TSS: TSS ADDED: ADDED:
GPD ppm ppm ppm gal lbs
08/01/00 1914 228 120.0 6720 0 0 I 08/02/00 0 7920 1 2
08/03/00 1875 243 120 9180 0 0
08/04/00 0 8300 0 0 I 08/05/00 2030 268 950.0 2260 0 0
08/06/00 0 1 1
08/07/00 0 0 0
08/08/00 2030 314 80 7760 0 0 I 08/09/00 0 0 0
08/10/00 2443 282 20 9180 0 0
08/11/00 0 0 0 I 08/12/00 2371 274 24 7460 0 0
08/13/00 0 1 0
08/14/00 2494 294 200 6800 0 0
08/15/00 0 0 0 I 08/16/00 1875 403 320 7780 0 0
08/17/00 0 0 0
08/18/00 2040 365 320 9160 0 0 I 08/19/00 0 1 0
08/20/00 2333 413 240 6160 1 0
08/21/00 0 1 0 I 08/22/00 2090 360 360 8440 0 0
08/23/00 0 0 0
08/24/00 1875 420 200 7560 0 0
08/25/00 0 I 08/26/00 2048 318 270 7700 0 0
08/27/00 0 1
08/28/00 2348 325 190 9000 0 0 I 08/29/00 0 0 0
08/30/00 2360 330 170 7400 1 1
08/31 /00 0 0 0
AVG: 1036 322 239 7575 0 0 I
MAX: 2494 420 950 9180 2
MIN: 0 228 20 2260 0 0 I DID NOT PROCESS SBR.
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I GROUNDWATER MONTHLY MONITORIN(
INNER TIER CARBON FILTER EFFLUENT #8 ITEF
PAGE NO. 7 I AUGUST.2000
DATE: PH: COD: TOG: TSS:
pH ppm ppm ppm
I 08/01/00
08/02/00
I 08/03/00 8.7 97 12 80
08/04/00
08/05/00
08/06/00
I 08/07/00
08/08/00 8.6 227 16
08/09/00
I 08/10/00
08/11/00
08/12/00
08/13/00
I 08/14/00
08/15/00
08/16/00 8.0 291 19
I 08/17/00
08/18/00
08/19/00
08/20/00
I 08/21/00
08/22/00
08/23/00
I 08/24/00 8.4 385 16
08/25/00
08/26/00
I 08/27/00
08/28/00
08/29/00
08/30/00 8.5 164 10
I 08/31/00
AVG: 8.4 233 14 80
I MAX: 8.7 385 19 80
MIN: 8.0 97 10 80
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INNER TIER I DAILY FLOW
SEPT. I
2000 IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9
09/01/00 30 26 62 34 272 25 78 357 577 I
09/02/00 61 25 116 30 180 17 77 356 555
09/03/00 36 21 104 433 166 10 67 314 506
09/04/00 32 25 67 51 181 23 75 369 4 I I 09/05/00 30 25 63 57 175 7 75 425 5
09/06/00 31 24 57 58 179 44 77 451 533
09/07/00 34 23 69 55 181 27 79 470 674 I 09/08/00 33 15 62 64 182 41 79 508 677
09/09/00 33 27 62 59 186 35 81 518 689
09/10/00 32 23 59 59 186 40 80 529 670
09/11 /00 31 24 59 63 193 20 82 551 700 I 09/12/00 32 14 60 70 190 14 83 600 739
09/13/00 51 27 54 65 131 18 74 294 274
09/14/00 53 24 58 80 157 19 84 347 718
09/15/00 51 24 62 81 136 18 88 354 743 I 09/16/00 48 19 56 74 181 2 78 299 660
09/17/00 43 8 52 69 207 5 70 260 643
09/18/00 so 44 60 76 223 0 89 321 497
09/19/00 31 16 38 so 158 4 54 200 471 I 09/20/00 44 27 60 62 218 6 66 275 29
09/21/00 49 26 60 70 208 4 91 317 35
09/22/00 51 25 87 159 204 89 88 324 618
09/23/00 51 24 92 141 195 97 87 320 733 I 09/24/00 46 24 62 53 193 97 86 313 4
09/25/00 48 24 64 54 162 96 91 322 51
09/26/00 45 23 57 55 101 49 17 321 6 I 09/27/00 46 24 63 58 79 43 8 324 798
09/28/00 45 8 59 58 64 59 6 321 791
09/29/00 47 25 59 59 202 99 91 519 168
09/30/00 43 24 58 61 227 113 112 526 0 I
AVG: 42 23 65 79 177 37 74 380 459 I TOTAL: 1257 688 1941 2358 5317 1121 2213 11405 13768
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GROUNDWATER MONTHLY MONITORING:
RAINFALL DATA
SEPT 2000
DATE INCHES/DAY
09/01/00 0.90
09/02/00 3.30
09/03/00 0.10
09/04/00 0.00
09/05/00 0.00
09/06/00 0.00
09/07/00 0.00
09/08/00 o.oo
09/09/00 o.oo
09/10/00 o.oo
09/11/00 0.00
09/12/00 0.00
09/13/00 0.00
09/14/00 0.00
09/15/00 0.00
09/16/00 0.00
09/17/00 0.00
09/18/00 0.80
09/19/00 0.00
09/20/00 0.20
09/21/00 0.10
09/22/00 1.50
09/23/00 o.oo
09/24/00 0.00
09/25/00 0.10
09/26/00 0.00
09/27/00 0.00
09/28/00 o.oo
09/29/00 0.00
09/30/00 0.00
TOTAL 7.00
23
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
ACTION
DATE WELL# PROBLEM DATE ACTION
9/6/00 #6 LOW FLOW 9/6/00 REPLACED EXHUSTER
916100 #9 LOW FLOW 9/6/00 CLEANED PROBE
9/13/00 #1 LOW FLOW 9/13/00 ADJUSTED CONTROLS
9/13/00 #8 LOW FLOW 9/13/00 REPLACED WATER LINE,METER & PUMP
9/13/00 #2 LOW FLOW 9/13/00 RESET PUMP
9/22/00 #6 LOW FLOW 9/22/00 REPLACE PUMP & METER
9/22/00 #9 LOW FLOW 9/22/00 CLEANED PROBE
9/25/00 #9 LOW FLOW 9/25/00 CLEANED PROBE
9/26/00 #9 LOW FLOW 9/26/00 RESET PUMP
9/29/00 #2 LOW FLOW 09/29/00 PULLED PUMP FREED CHECK BALLS
9/29/00 #2 LOW FLOW 09/29/00 CLEANED STRAINER
9/29/00 #5 LOW FLOW 09/29/00 REPLACE PUMP& CLEANED STRAINER
9/29/00 #6 LOW FLOW 09/29/00 ADJUSTED CONTROLS
9/29/00 #7 LOW FLOW 09/29/00 REPLACED PUMP & CLEANED STRAINER
24
MECHANIC
MAX &P.P.
MAX&P.P.
MAX &P.P.
MAX&P.P.
MAX&P.P.
MAX&P.P.
MAX&P.P.
MAX &P.P.
MAX
MAX
MAX
MAX
MAX
MAX
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I DAILY REFERENCE SHEET:
I DATE: IT. EQ. PLT. DEC. DEC. WAS MIX MIX MIX NIT PHOS MIX F/M
SEPT. INF. TNK. SEP. LIQ LIQ LIQ ADD ADD LIQ WAS 5/DAY
2000 COD. COD. COD. COD. TSS. TSS MLSS !':!!I PHOS GALS LBS SET. GALS F/M AVG.
I 1 3460 3380 3540 332 21 8440 940 110 20 0 0 50 25 0.33
2 3340 3690 1056 96 19 1 0 50 0 0.00
3 2730 3670 3620 378 220 3810 1016 119 22 0 0 50 25 0.32
4 2750 2730 1096 131 16.5 0 50 0 0.00
I 5 6320 4000 3690 391 150 9240 1064 111 15.1 0 50 25 0.31 0.19
6 6860 4320 1060 89 16.6 1 1 50 0 0.00 0.12
7 3350 3600 3730 365 210 5600 1072 111 23.3 0 0 50 25 0.31 0.19
8 3580 3490 1108 103 19.3 1 1 50 0 0.00 0.12
9 4470 3500 4150 285 140 9560 1028 116 26.3 0 0 50 25 0.36 0.20
I 10 3550 3260 1172 137 26 0 0 50 0 0.00 0.13
11 3530 3430 3380 251 160 7620 1068 105 20.1 0 0 50 25 0.28 0.19
12 3490 3440 3860 329 270 11020 1164 125 15.5 0 0 50 25 0.29 0,19
13 3500 3540 1156 70 75 1 80 0 0.00 0.19
I 14 4240 3620 3410 281 100 8600 1112 103 20.1 0 0 50 25 0.27 0.17
15 4260 3950 1160 90 14.5 1 1 50 0 0.00 0.17
16 3310 3860 3580 259 150 9600 1064 103 37 0 50 50 0.30 0.17
17 3310 4020 1168 133 27.4 0 0 50 0 0.00 0.11
18 3490 3610 4070 275 130 9060 1104 120 24.5 0 0 50 25 0.33 0.18
I 19 4100 3590 1252 101 17.6 0 0 50 0 0.00 0.13
20 3990 3010 2900 250 110 12660 1140 109 25.5 0 0 50 25 0.23 0.17
21 6960 4290 1272 111 22.5 0 0 50 0 0.00 0.11
22 7320 4740 3340 252 140 9820 1172 97 23.2 1 50 25 0.25 0.16
I 23 3140 4580 1316 97 20.0 1 2 50 0 0.00 0.10
24 4400 4180 4850 248 130 7880 1216 122 30.3 0 0 50 25 0.35 0.17
25 7620 4510 1264 113 25.0 0 0 50 0 0.00 0.12
26 8330 4590 3640 244 100 8000 1264 133 22.5 0 0 50 25 0,26 0.17
27 6820 4680 1288 97 17.6 1 2 50 0 0.00 0.12
I 28 3080 4430 4290 174 60 8160 1264 145 36.0 0 0 50 25 0.30 0.18
29 4110 3790 1376 95 25.0 0 0 50 0 0.00 0.11
30 7380 4450 4080 245 170 9310 1316 90 26.5 1 0 80 25 0,28 0.17
I AVG: 4560 3865 3537 268 133 8140 1158 109.4 22.1 0 0 52 14 0.16
MAX: 8330 4740 4850 391 270 12660 1376 145.0 37.0 1 2 80 50 0.36
MIN: 2730 2730 0 0 0 0 940 70.0 7.5 0 0 50 0 0.00
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INNER TIER COMBINED INFLUENT #2 ITCI
PAGE NO.1
SEPT.2000 I DATE: FLOW: PH: COD: TSS: TOG:
GPD pH ppm ppm ppm
09/01/00 1461 5.3 3460 19 I
09/02/00 1417 5.2 3340 8
09/03/00 1657 5.5 2730 18 I 09/04/00 827 5.2 2750 13
09/05/00 862 5.2 6320 22
09/06/00 1454 5.2 6860 26
09107/00 1612 5.4 3350 7 1360 I 09/08/00 1661 5.4 3580 8
09/09/00 1690 5.4 4470 34
09/10/00 1678 5.4 3550 10 I 09/11/00 1723 5.5 3530 11
09/12/00 1802 5.5 3490 29 1350
09/13/00 988 5.3 3500 9
09/14/00 1540 5.3 4240 13 I 09/15/00 1557 5.3 4260 2
09/16/00 1417 5.2 3310 5
09/17/00 1557 5.2 3140 4 I 09/18/00 1360 5.3 3490 11
09/19/00 1022 5.3 4100 5
09/20/00 787 5.3 3990 10 1310
09/21/00 860 5.1 6960 1 I 09/22/00 1645 5.2 7320 9
09/23/00 1740 5.3 3140 15
09/24/00 878 5.3 4400 10 I 09/25/00 912 5.2 7620 6
09/26/00 674 5.1 8330 4 2520
09/27/00 1443 5.1 6820 15 I 09/28/00 1411 5.2 3080 14
09/29/00 1269 5.2 4110 3
09/30/00 1164 5.2 7380 35 I
AVG: 1336 5.3 4554 13 1635
MAX: 1802 5.5 8330 35 2520 I MIN: 674 5.1 2730 1 1310
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I GROUNDWATER MONTHLY MONITORING:
INNER TIER EQUALIZATION TANK: ITEQT
I PAGE NO. 2
SEPT.2000
DATE: PH: COD: OT WATER ADDED
I
pH ppm gal
09/01/00 7.7 3380
09/02/00 7.7 3690
I 09/03/00 7.7 3670
09/04/00 7.6 2730
09/05/00 7.6 4000
I 09/06/00 7.7 4320
09/07/00 7.7 3600 263
09/08/00 7.9 3490
09/09/00 7.7 3500
I 09/10/00 7.7 3260
09/11/00 7.7 3430
09/12/00 7.8 3440 488
I 09/13/00 7.8 3540
09/14/00 7.7 3620
09/15/00 7.7 3950
09/16/00 7.7 3860
I 09/17/00 7.8 4020
09/18/00 7.6 3610
09/19/00 7.7 3590
I 09/20/00 7.7 3010
09/21/00 7.6 4290
09/22/00 7.7 4740
I 09/23/00 7.8 4580
09/24/00 7.5 4180
09/25/00 7.7 4510
09/26/00 11.2 4590 375
I 09/27/00 7.7 4680
09/28/00 7.7 4430 190
09/29/00 7.7 3790
I 09/30/00 7.5 4450
AVG: 7.8 3865 329
I MAX: 11.2 4740 488
MIN: 7.5 2730 190
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GROUNDWATER MONTHLY MONITORING: I
AFTER PLATE SEPARATOR BEFORE SBR: SBRI
PAGE NO. 3 I SEPT.2000
DATE: PH: COD: TSS:
pH ppm ppm I I
09/01/00 7.1 3540 40
09/02/00
09/03/00 7.1 3620 60 I 09/04/00
09/05/00 7.2 3690 80
09/06/00 I 09/07/00 6.7 3730 116
09/08/00
09/09/00 6.3 4150 8
09/10/00 I 09/11/00 6.3 3380 4
09/12/00 6.4 3860 12
09/13/00 I 09/14/00 5.8 3410 4
09/15/00
09/16/00 7.1 3580 16
09/17/00 I 09/18/00 5.9 4070 8
09/19/00
09/20/00 5.8 2900 28 I 09/21/00
09/22/00 6.1 3340 8
09/23/00 I 09/24/00 5.9 4850 48
09/25/00
09/26/00 5.7 3640 16
09/27/00 I 09/28/00 6.5 4290 20
09/29/00
09/30/00 5.8 4080 20 I
AVG: 6.4 3758 31
MAX: 7.2 4850 116 I MIN: 5.7 2900 4
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28 I
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I GROUNDWATER MONTHLY MONITORING:
SBR MIXED LIQUOR: SBRML
I PAGE NO.4
SEPT.2000 SETT. SLUDGE 5/DAY
DATE: PH: NH3N: PO4: DO: MLSS: MLVSS: SOLIDS: WASTED F/M: F/M:
pH ppm ppm ppm ppm ppm ml/I gal ratio ratio
I 09/01/00 8.4 110 20.0 4.0 940 50 25 0.33
09/02/00 8.4 96 19.0 3.3 1056 50 0 0.00
I 09/03/00 8.5 119 22.0 3.6 1016 50 25 0.32
09104100 8.4 131 16.5 3.4 1096 50 0 0.00
09/05/00 8.4 111 15.1 3.1 1064 716 50 25 0.31 0.19
I 09/06/00 8.4 89 16.6 2.3 1060 50 0 0.00 0.12
09/07/00 8.7 111 23.3 3.5 1072 50 25 0.31 0.19
09/08/00 8.5 103 19.3 3.1 1108 50 0 0.00 0.12
09/09/00 8.5 116 26.3 2.7 1028 50 25 0.36 0.20
I 09/10/00 8.7 137 26.0 3.1 1172 50 0 0.00 0.13
09/11/00 8.7 105 20.1 3.0 1068 50 25 0.28 0.19
09/12/00 8.5 125 15.5 2.5 1164 772 50 25 0.29 0.19
I 09/13/00 8.3 70 7.5 2.8 1156 80 0 0.00 0.19
09/14/00 8.4 103 20.1 3.1 1112 50 25 0.27 0.17
09/15/00 8.3 90 14.5 3.0 1160 50 0 0.00 0.17
09/16/00 8.4 103 37.0 3.1 1064 50 50 0.30 0.17
I 09/17/00 8.7 133 27.4 3.1 1168 50 0 0.00 0.11
09/18/00 8.6 120 24.5 3.4 1104 50 25 0.33 0.18
09/19/00 8.3 101 17.6 2.3 1252 892 50 0 0.00 0.13
I 09/20/00 8.4 109 25.5 4.2 1140 50 25 0.23 0.17
09/21/00 8.4 111 22.5 2.2 1272 50 0 0.00 0.11
09122100 8.4 97 23.2 2.0 1172 50 25 0.25 0.16
09/23/00 8.7 97 20.0 4.0 1316 50 0 0.00 0.10 I 09/24/00 8.6 122 30.3 3.8 1216 50 25 0.35 0.17
09/25/00 8.4 113 25.0 2.8 1264 50 0 0.00 0.12
09/26/00 8.6 133 22.5 3.4 1264 876 50 25 0.26 0.17
I 09/27/00 8.5 97 17.6 3.0 1288 50 0 0.00 0.12
09/28/00 8.5 145 36.0 5.2 1264 50 25 0.30 0.18
09/29/00 8.5 95 25.0 3.9 1376 50 0 0.00 0.11
I 09/30/00 8.5 90 26.5 5.7 1316 80 25 0.28 0.17
AVG: 8.5 109 22 3 1158 814 52 14 0.16 0.16
I MAX: 8.7 145 37 6 1376 892 80 50 0.36 0.20
MIN: 8.3 70 8 2 940 716 50 0 0.00 0.10
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GROUNDWATER MONTHLY MONITORING: I
SBR EFFLUENT:(DECAN1) #4 SBRE
PAGE NO. 5 I SEPT.2000 WAS. NH3N PHOS.
DATE: FLOW: COD: TSS: TSS ADDED: ADDED:
GPO ppm ppm ppm gal lbs
09/01/00 2311 332 210 8440 0 0 I
09/02/00 0 0
09/03/00 2822 378 220 3810 0 0 I 09/04/00 0 1 0
09/05/00 2498 391 150 9240 0 1
09/06/00 0 1 1 I 09/07/00 2227 365 210 5600 0 0
09/08/00 0 1 1
09/09/00 1795 285 140 9560 0 0
09/10/00 0 0 0 I 09/11/00 2472 251 160 7620 0 0
09/12/00 2325 329 270 11020 0 0
09/13/00 0 I 09/14/00 2267 281 100 8600 0 0
09/15/00 0 1 1
09/16/00 2194 259 150 9600 1 0
09/17/00 0 0 0 .I 09/18/00 2396 275 130 9060 0 0
09/19/00 0 0 0
09/20/00 2507 250 110 12660 0 0 I 09/21/00 0 0 0
09/22/00 2415 252 140 9820 1 1
09/23/00 0 1 2
09/24/00 2259 248 130 7880 0 0 I 09/25/00 0 0 0
09/26/00 2445 244 100 8000 0 0
09/27/00 0 1 2 I 09/28/00 2336 174 60 8160 0 0
09/29/00 0 0 0
09/30/00 2156 245 170 9310 0 I
AVG: 1248 285 153 8649 0 0
MAX: 2822 391 270 12660 2 I MIN: 0 174 60 3810 0 0
DID NOT PROCESS SBR.
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I GROUNDWATER MONTHLY MONITORIN(
INNER TIER CARBON FILTER EFFLUENT #8 ITEF
I PAGE NO. 7
SEPT.2000
DATE: PH: COD: TOC: TSS:
pH ppm ppm ppm
I 09/01/00
09/02/00
I 09/03/00
09/04/00
09/05/00
I 09/06/00
09/07/00 8.6 295 19 150
09/08/00
09/09/00
I 09/10/00
09/11/00
09/12/00 8.6 272 14
I 09/13/00
09/14/00
09/15/00
09/16/00
I 09/17/00
09/18/00
09/19/00
I 09/20/00 8.4 183 15
09/21/00
09/22/00
I 09/23/00
09/24/00
09/25/00
09/26/00 8.0 278 15
I 09/27/00
09/28/00
09/29/00
I 09/30/00
AVG: 8.4 257 16 150
I MAX: 8.6 295 19 150
MIN: 8.0 183 14 150
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INNER TIER I DAILY FLOW
OCT. I
2000 IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9 I 10/01 /00 42 24 61 64 219 107 111 525 0
10/02/00 41 22 59 70 216 126 105 511 266
10/03/00 43 27 59 72 212 129 105 528 0 I 10/04/00 42 17 59 76 225 131 102 528 0
10/05/00 42 22 60 81 228 131 104 118 250
10/06/00 37 22 59 83 241 123 104 448 107
10/07/00 10 1 60 87 230 66 110 495 0 I 10/08/00 0 0 58 86 207 25 108 464 0
10/09/00 0 29 60 73 210 36 109 486 21
10/10/00 37 22 60 107 205 31 109 478 320
10/11/00 36 22 53 83 192 26 96 402 291 I 10/12/00 37 21 59 97 211 28 110 494 360
10/13/00 35 22 59 90 190 30 101 409 362
10/14/00 73 42 59 91 216 33 107 372 365
10/15/00 35 21 58 90 208 50 99 349 359 I 10/16/00 35 18 60 97 207 64 101 320 455
10/17/00 36 39 116 189 395 224 200 640 686
10/18/00 35 20 49 94 196 129 99 349 343 I 10/19/00 34 20 67 93 193 89 95 336 344
10/20/00 35 21 58 97 193 87 95 329 357
10/21/00 35 20 59 90 227 96 91 314 365
10/22/00 35 21 61 90 234 146 94 144 442 I 10/23/00 33 23 62 86 221 86 92 100 383 I
10/24/00 34 319 62 87 229 39 97 82 539
10/25/00 31 769 63 84 229 20 97 470 585
10/26/00 37 72 64 86 223 33 98 522 478 I 10/27/00 3 33 61 85 190 30 93 496 357
10/28/00 0 22 64 93 191 37 100 501 465
10/29/00 0 6 63 87 190 9 109 488 575
10/30/00 30 14 63 83 194 20 107 472 514 I 10/31/00 34 0 63 83 198 35 108 470 500
AVG: 31 56 62 89 217 71 105 408 325 I
TOTAL: 957 1731 1918 2774 6720 2216 3256 12640 10089
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GROUNDWATER MONTHLY MONITORING:
RAINFALL DATA
OCT 2000
DATE INCHES/DAY
10/01/00 o.oo
10/02/00 0.00
10/03/00 0.00
10/04/00 0.00
10/05/00 0.00
10/06/00 o.oo
10/07/00 o.oo
10/08/00 0.00
10/09/00 0.00
10/10/00 0.00
10/11/00 0.00
10/12/00 0.00
10/13/00 0.00
10/14/00 o.oo
10/15/00 o.oo
10/16/00 o.oo
10/17/00 o.oo
10/18/00 o.oo
10/19/00 o.oo
10/20/00 o.oo
10/21/00 o.oo
10/22/00 o.oo
10/23/00 o.oo
10/24/00 o.oo
10/25/00 o.oo
10/26/00 o.oo
10/27/00 0.00
10/28/00 o.oo
10/29/00 o.oo
10/30/00 o.oo
10/31/00 o.oo
TOTAL 0.00
33
Quarterly O&M Plan Checklist-HNA Holdings, lnc./Shelby, NC
c,,,
.i,,.
Outer Tier Well
OT-2R
OT-3
OT-4
OT-5
OT-6
OT-6A
OT-7
OT-8
Ground-Water
Treatment Sys.
- - -
Open Sample
Port
X
X
X
X
X
X
X
X
Energize
AS Blower
Y-V-1008
-
Energize Verify De-energize Close Sample
Pump Discharge Pump Port
X X X X
X X X X
X X X X
X X X X
X X X X
X X X X
X X X X
X X X X
Energize Energize Energize Energize
Transfer Pump Transfer Pump Transfer Pump Transfer Pump
Y-P-1007A Y-P-1007B Y-P-1008A Y-P-1008B
- - -- -
Form Completed by: TONY BRYANT
Date: 1 0/2/00
Verily Heater Secure Well
Operation Vault Comments
X X
X X
X X
X X
X X
X X
X X
X X
Comments
------ - -- -
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MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
ACTION
DATE WELL# PROBLEM DATE ACTION
10/2/00 #9 low flow 10/2/00 reset ctrls &relaced line to header
10/5/00 #9 low flow 10/5/00 reset ctrls & adj. Water flow
10/5/00 #8 low flow 10/5/00 replaced pump
10/6/00 #8 low flow 10/6/00 cleaned line &screen
10/26/00 #6 low flow 10/26/00 replacedexhauster &adjusted controler
10/26/00 #2 low flow 10/26/00 replaced pump wirh rebuilt pump
10/30/00 #6 lowfiow 10/30/00 resetcontrols
10/30/00 #2 low flow 10/30/00 reset pump
10/30/00 #1 low flow 10/30/00 worked on control block & loose air fitting
35
MECHANIC
max & p.p.
max& p.p.
max & p.p.
max & p.p.
max & p.p.
max& p.p.
max & p.p.
max & p.p.
max & p.p.
I
I DAILY REFERENCE SHEET:
DATE: IT. EQ. PLT. DEC. DEC. WAS MIX MIX MIX NIT PHOS MIX · F/M I OCT. INF. TNK. SEP. LIQ LIQ LIQ ADD ADD LIQ WAS 5/DAY
2000 COD. COD. COD. COD. TSS. TSS MLSS NIT PHOS GALS LBS SET. GALS F/M AVG.
1 6950 4980 1328 120 23.5 0 0 80 0 0.00 I 2 6110 1760 4420 246 200 9460 1356 88 20.2 1 2 80 25 0.29
3 5970 4860 1460 105 25.2 0 0 70 0 0.00
4 5290 3760 4640 278 140 6500 1364 138 31 0 0 80 25 0.30
5 6900 5070 1460 97 22.1 3 0 80 0 0.00 0.12 I 6 8420 5040 4770 316 210 9260 1328 90 24.2 0 0 80 25 0.32 0.18
7 5980 4650 1324 109 21.5 0 0 100 0 0.00 0.12
8 7070 6150 5350 342 350 9460 1368 105 32.1 1 1 90 60 0.35 0.19
9 5870 5640 1316 82 25 80 0 0.00 0.13
10 3340 9300 1276 140 39 0 0 80 0 0.00 0.13 I 11 4430 4230 4270 316 140 6300 1320 136 41.5 0 0 70 25 0.29 0.13
12 3930 3880 1308 91 30.3 0 0 70 0 0.00 0.13
13 3980 3680 3980 383 170 7240 1432 86 31.4 1 70 25 0.25 0.11
14 3260 3200 1200 110 32.3 0 0 70 0 0.00 0.11 I 15 3070 3040 3350 263 140 6800 1276 111 33.5 0 0 70 25 0 23 0,15
16 4040 4220 1204 85 23.3 0 0 70 0 0.00 0.10
17 4950 4280 4830 402 230 7900 1220 83 25.5 2 0 100 25 0.35 0.17
18 5030 4040 1348 111 22.5 0 0 80 0 0.00 0.12
19 4020 5070 3970 430 240 8630 1392 114 20.2 0 0 60 25 0.25 0.17 I 20 4860 4490 1272 78 18.6 0 0 60 0 0.00 0.12
21 4180 4400 4320 495 320 9800 1252 97 30.7 1 0 80 54 0.31 0.18
22 4220 4210 1284 105 25.2 0 0 80 0 0.00 0.11
23 5520 4140 4940 550 320 7600 1380 116 27.5 0 80 81 0.32 0.18 I 24 4220 3970 1612 108 20.0 1 0 150 0 0.00 0.12
25 3200 3950 4380 537 330 5130 1596 135 22.5 0 0 60 25 0.24 0.17
26 3380 4180 1280 92 14.7 2 60 0 0.00 0.11
27 4260 3960 4210 595 440 9400 1276 110 25.0 0 0 60 25 0.29 0.17
28 3120 3240 1532 111 25.0 0 0 50 0 0.00 0.11 I 29 2090 3080 2840 659 300 1660 1420 93 23.0 0 0 50 100 0.18 0.14
30 2080 2550 3030 702 400 6620 1852 98 17.0 1 2 50 100 0.15 0.12.
31 4690 2430 1304 126 27.6 0 0 50 100 0.00 0.12
AVG: 4659 4240 3724 383 231 6574 1366 105.5 25.8 0 0 75 24 0.13 I MAX: 8420 9300 5350 702 440 9800 1852 140.0 41.5 3 2 150 100 0.35
MIN: 2080 1760 0 0 0 0 1200 78.0 14.7 0 0 50 0 0.00
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INNER TIER COMBINED INFLUENT #2 ITCI
I PAGE N0.1
OCT.2000
DATE: FLOW: PH: COD: TSS: TOC:
I
GPO pH ppm ppm ppm
10/01/00 1153 5.2 6950 14
10/02/00 1416 5.1 6110 10
I 10/03/00 1175 5.2 5970 34
10/04/00 1180 5.2 5290 13 2220
10/05/00 1036 5.2 6900 15
I
10/06/00 1224 5.1 8420 14
10/07/00 1059 5.2 5980 14
10/08/00 948 5.1 7070 156
10/09/00 1024 5.3 5870 85
I 10/10/00 1369 5.4 3340 12
10/11/00 1201 5.4 4430 28 2300
10/12/00 1417 5.5 3930 40
I 10/13/00 1298 5.5 3980 30
10/14/00 1358 5.5 3260 6
10/15/00 1269 5.5 3070 6
10/16/00 1357 5.4 4040 5
I 10/17/00 2525 5.4 4950 4
10/18/00 1314 5.5 5030 3
10/19/00 1271 5.5 4020 8 1320
I 10/20/00 1272 5.3 4860 11
10/21/00 1297 5.3 4180 8
10/22/00 1267 5.4 4220 6
I 10/23/00 1086 5.4 5520 3
10/24/00 1488 5.2 4220 8
10/25/00 2348 5.3 3200 89 1280
10/26/00 1613 5.5 3380 36
I 10/27/00 1348 5.6 4260 46
10/28/00 1473 5.6 3120 21
10/29/00 1527 5.6 2090 21
I 10/30/00 1497 5.6 2080 29
10/31/00 1491 5.5 4690 43
AVG: 1365 5.4 4659 26 1780
I MAX: 2525 5.6 8420 156 2300
MIN: 948 5.1 2080 3 1280
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GROUNDWATER MONTHLY MONITORING: I
INNER TIER EQUALIZATION TANK: ITEQT
PAGE NO. 2 I OCT.2000
DATE: PH: COD: OT WATER ADDED
pH ppm gal
I 10/01/00 7.7 4980
10/02/00 7.5 4760 225
10/03/00 7.7 4860 I 10/04/00 7.6 3760
10/05/00 7.7 5070
10/06/00 7.6 5040 375
10/07/00 7.7 4650 I 10/08/00 7.5 6150
10/09/00 7.7 5640
10/10/00 7.7 4300 I 10/11/00 7.5 4230
10/12/00 7.7 3880
10/13/00 7.5 3680 I 10/14/00 7.8 3200
10/15/00 7.7 3040
10/16/00 7.7 4220
10/17/00 7.7 4280 I 10/18/00 7.9 4040
10/19/00 7.8 5070
10/20/00 7.9 4490 I 10/21/00 7.8 4400
10/22/00 7.8 4210
10/23/00 7.9 4140
10/24/00 8.1 3970 I 10/25/00 7.9 3950
10/26/00 7.9 4180
10/27/00 7.9 3960 I 10/28/00 7.9 3240
10/29/00 8.1 3080
10/30/00 8.1 2550 I 10/31/00 8.4 2430
AVG: 7.8 4176 300
MAX: 8.4 6150 375 I MIN: 7.5 2430 225
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I GROUNDWATER MONTHLY MONITORING:
AFTER PLATE SEPARATOR BEFORE SBR: SBRI
I PAGE NO. 3
OCT.2000
DATE: PH: COD: TSS:
pH ppm ppm
I 10/01/00
10/02/00 5.8 4420 12
I 10/03/00
10/04/00 5.6 4640 4
10/05/00
10/06/00 5.6 4770 20
I 10/07/00
10/08/00 6.6 5350 28
10/09/00
I 10/10/00
10/11/00 6.2 4270 28
10/12/00
I 10/13/00 7.0 3980 4
10/14/00
10/15/00 5.7 3350 4
10/16/00
I 10/17/00 5.7 4830 8
10/18/00
10/19/00 6.1 3970 4
I 10/20/00
10/21/00 7.3 4320 28
10/22/00
10/23/00 6.1 4940 8
I 10/24/00
10/25/00 6.1 4380 16
10/26/00
I 10/27/00 6.3 4210 40
10/28/00
10/29/00 6.9 2840 24
I 10/30/00 6.4 3030 8
10/31/00
AVG: 6.2 4220 16
I MAX: 7.3 5350 40
MIN: 5.6 2840 4
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GROUNDWATER MONTHLY MONITORING: I
SBR MIXED LIQUOR: SBRML
PAGE NO.4 I OCT.2000 SETT. SLUDGE 5/DAY
DATE: PH: NH3N: PO4: DO: MLSS: MLVSS: SOLIDS: WASTED F/M: F/M:
pH ppm ppm ppm ppm ppm ml/I gal ratio ratio
10/01 /00 8.5 120 23.5 5.6 1328 80 0 0.00 I
10/02/00 8.5 88 20.2 4.2 1356 80 25 0.29
10/03/00 8.5 105 25.2 5.4 1460 1048 70 0 0.00 I 10/04/00 8.5 138 31.0 2.2 1304 80 25 0.32
10/05/00 8.5 97 22.1 5.2 1460 80 0 0.00 0.12
10/06/00 8.6 90 24.2 3.8 1328 80 25 0.32 0.19
10/07/00 8.5 109 21.5 3.7 1324 100 0 0.00 0.13 I 10/08/00 8.5 105 32.1 3.7 1368 90 60 0.35 0.20
10/09/00 8.5 82 25.0 5.1 1316 80 0 0.00 0.13
10/10/00 8.6 140 39.0 5.7 1276 908 80 0 0.00 0.13 I 10/11/00 8.5 136 41.5 5.7 1320 70 25 0.29 0.13
10/12/00 8.5 91 30.3 5.1 1308 70 0 0.00 0.13
10/13/00 8.6 86 31.4 5.7 1432 70 25 0.25 0.11
10/14/00 8.6 110 32.3 5.2 1200 70 0 0.00 0.11 I 10/15/00 8.5 111 33.5 5.2 1276 70 25 0.23 0.15
10/16/00 8.5 85 23.3 5.4 1204 70 0 0.00 0.10
10/17/00 8.6 83 25.5 4.9 1220 870 100 100 0.35 0.17 I 10/18/00 8.6 111 22.5 4.7 1348 80 0 0.00 0.12
10/19/00 8.6 114 20.2 6.0 1392 60 25 0.25 0.17
10/20/00 8.7 78 18.6 5.1 1272 60 0 0.00 0.12 I 10/21 /00 8.6 97 30.7 5.6 1252 80 54 0.31 0.18
10/22/00 8.7 105 25.5 5.2 1284 80 0 0.00 0.11
10/23/00 8.6 116 27.5 5.9 1380 80 81 0.32 0.18
10/24/00 8.6 108 20.0 5.7 1612 1092 150 0 0.00 0.12 I 10/25/00 8.5 135 22.5 4.4 1596 60 25 0.24 0.17
10/26/00 8.5 92 14.7 4.2 1280 60 0 0.00 0.11
10/27/00 8.7 110 25.0 5.8 1276 60 25 0.29 0.17 I 10/28/00 8.5 111 25.0 4.7 1532 50 0 0.00 0.11
10/29/00 8.5 93 23.0 5.2 1420 50 100 0.18 0.14
10/30/00 8.6 98 17.0 5.2 1852 50 100 0.15 0.12
10/31/00 8.7 126 27.6 5.3 1304 944 50 100 0.00 0.12 I
AVG: 8.6 105 26 5 1364 972 75 26 0.13 0.14
MAX: 8.7 140 42 6 1852 1092 150 100 0.35 0.20 I MIN: 8.5 78 15 2 1200 870 50 0 0.00 0.10
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I GROUNDWATER MONTHLY MONITORING:
SBR EFFLUENT:(OECANl) #4 SBRE
I PAGE NO. 5
OCT.2000 WAS. NH3N PHOS.
DATE: FLOW: COO: TSS: TSS ADDED: ADDEO:
I
GPO ppm ppm ppm gal lbs
10/01/00 0 0 0
10/02/00 2237 246 200 9460 1 2
I 10/03/00 0 0 0
10/04/00 1884 278 140 6500 0 0
10/05/00 0 0 0
I 10/06/00 1947 316 210 9260 0 0
10/07/00 0 0 0
10/08/00 1883 342 350 9460 1
10/09/00 0
I 10/10/00 0 0 0
10/11/00 1983 316 140 6300 0 0
10/12/00 0 0 0
I 10/13/00 2372 383 170 7240 1 1
10/14/00 0 0 0
10/15/00 2438 263 140 6800 0 0
I 10/16/00 0 0 0
10/17/00 2354 402 230 7960 2 0
10/18/00 0 0 0
10/19/00 2060 430 240 8620 0 0
I 10/20/00 0 0 0
10/21/00 2123 495 320 9800 0
10/22/00 0 0
I 10/23/00 2215 550 320 7600 0
10/24/00 0 1 0
10/25/00 2050 537 330 5130 0 0
10/26/00 0 1 2
I 10/27/00 1689 595 440 9400 0 0
10/28/00 0
10/29/00 2454 659 300 1660 0 0
I 10/30/00 2442 702 400 6620 2
10/31/00 0 0 0
I
AVG: 1036 434 262 7454 0 0
MAX: 2454 702 440 9800 2 2
MIN: 0 246 140 1660 0 0
• DID NOT PROCESS SBR .
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GROUNDWATER MONTHLY MONITOR IN( I
INNER TIER CARBON FILTER EFFLUENT #8 ITEF
PAGE NO. 7 I OCT.2000
DATE: PH: COD: TOC: TSS:
pH ppm ppm ppm
10/01/00 I
10/02/00
10/03/00 I 10/04/00 8.3 250 17 130
10/05/00
10/06/00
10/07/00 I 10/08/00
10/09/00
10/10/00 I 10/11/00 8.4 193 20
10/12/00
10/13/00 I 10/14/00
10/15/00
10/16/00
10/17/00 I 10/18/00
10/19/00 8.5 428 28
10/20/00 I 10/21/00
10/22/00
10/23/00
10/24/00 I 10/25/00 8.0 540 35
10/26/00
10/27/00 I 10/28/00
10/29/00
10/30/00 I 10/31/00
AVG: 8.3 353 25 130
MAX: 8.5 540 35 130 I MIN: 8.0 193 17 130
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I INNER TIER
DAILY FLOW
I NOV.
I 2000 IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9
11/01/00 31 27 55 74 176 85 90 417 317
11/02/00 33 27 58 84 189 83 108 465 352
I 11 /03/00 33 19 59 83 185 67 104 461 367
11/04/00 32 1 58 84 185 33 103 460 418
11/05/00 32 0 58 90 186 27 104 449 418
11/06/00 32 10 58 82 185 49 105 451 412
I 11/07/00 31 0 57 80 195 74 100 444 452
11/08/00 32 0 63 76 213 74 79 439 354
11/09/00 31 18 50 74 217 74 98 431 308
11/10/00 32 20 57 92 226 48 67 448 314
I 11/11/00 31 19 60 111 219 47 102 436 327
11/12/00 29 18 55 108 237 39 104 418 342
11/13/00 31 18 58 127 255 78 100 431 351
11/14/00 31 19 57 86 243 40 104 430 387
I 11/15/00 26 18 58 107 226 36 101 425 395
11/16/00 35 19 59 108 213 72 109 435 450
11/17/00 30 18 58 104 212 39 92 420 465
I 11/18/00 32 20 63 110 225 37 108 449 499
11/19/00 27 17 52 92 195 o 94 369 397
11 /20/00 0 0 0 0 0 o 0 0 0
11/21/00 30 18 58 107 219 o 103 396 484
I 11/22/00 29 19 59 98 216 o 103 395 495
11/23/00 28 16 54 90 180 0 88 367 474
11 /24/00 31 20 57 89 178 o 84 396 436
11/25/00 29 18 63 99 188 0 91 413 582
I 11/26/00 30 17 58 87 191 o 87 409 478
11/27/00 29 18 59 90 193 o 80 409 479
11 /28/00 30 17 59 90 200 0 95 382 480
11/29/00 29 17 59 88 198 o 90 383 486
I 11 /30/00 29 17 59 84 200 0 90 386 485
I AVG: 30 16 56 90 198 33 93 407 407
TOTAL: 885 465 1678 2694 5945 1002 2783 12214 12204
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GROUNDWATER MONTHLY MONITORING:
RAINFALL DATA
nov 2000 .
DATE INCHES/DAY
11/01/00 0.00
11/02/00 0.00
11/03/00 0.00
11/04/00 0.20
11/05/00 0.00
11/06/00 o.oo
11/07 /00 0.00
11/08/00 0.30
11/09/00 1.10
11/10/00 0.00
11/11/00 0.00
11/12/00 o.oo
11/13/00 0.40
11/14/00 o.oo
11/15/00 0.00
11/ 16 /00 0.30
11/17/00 0.05
11/18/00 o.oo
11/19/00 0.50
11/20/00 o.oo
11/21/00 0.00
11/22/00 0.00
11/23/00 0.00
11/24/00 0.50
11/25/00 0.70
11/26/00 0.00
11/27 /00 0.00
11/28/00 0.00
11/29/00 o.oo
11/30/00 0.00
TOTAL 4.05
44
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"""" c..n
- --
Well
OT-2R
OT-3
OT-4
OT-5
OT-6
OT-6A
OT-7
OT-8
-

-

-

-
Thermometer
Operational? ..
X
X
X
X
X
X
X
X
--

-

-

-
-

-

-
Monthly O&M Plan Checklist
HNA Holdings, Inc., Shelby, NC
Heat Lamp
Operational? ..
X
X
X
X
X
X
X
X
Other Operational Items/Comments
-

-

-

-
(.. Temperature and Heat Lamp checks October thru April only)
Form Completed by: __________ ...:T_,,O:,_NY::..:...;B::,Rc.:.Y-"ANT=~---------
Date: __________ __!_1 .,_1 /c._1,_,/--"0-"0'--------------
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
ACTION
DATE WELL# PROBLEM DATE ACTION
1116/00 #2 LOW FLOW 11/6100 RESET PUMP
1116/00 #6 NO FLOW 11/6100 EVERY CHECKED GOOD NO WATER
46
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MECHANIC
MAX&P.P.
MAX&P.P.
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DAILY REFERENCE SHEET:
I DATE: IT. EQ. PLT. DEC. DEC. WAS MIX MIX MIX NIT PHOS MIX FIM
NOV. INF. TNK. SEP. LIQ LIQ LIQ ADD ADD LIQ WAS 5/DAY
2000 COD. COD. COD. COD. TSS. TSS MLSS NII PHOS GALS LBS SET. GALS FIM AVG.
I 1 5020 3210 2670 603 550 10280 1604 145 27.5 0 0 50 100 0.15
2 4960 3960 1220 108 22.7 0 0 50 0 0.00
3 4630 3990 3880 618 320 11840 1142 91 18.3 2 50 100 0.30
4 4100 4550 1260 118 27.0 0 0 50 0 0.00
I 5 3710 4550 3600 840 540 11200 1012 118 27.9 0 0 50 100 0.32 0.15
6 5210 4050 1756 102 24.3 0 0 50 0 0.00 0.12
7 4500 4420 3930 651 310 2440 1512 108 22.6 0 0 50 100 0.23 0.17
8 3580 4110 4430 692 400 1290 1272 89 20.5 2 50 100 0.31 0.17
I 9 5060 3440 1848 101 29.7 0 50 0 0.00 0.17
10 5580 4650 4660 826 400 5960 1124 94 24.3 0 50 25 0.37 0.18
11 5100 4770 1200 115 16.0 1 50 0 0.00 0.18
12 5010 4830 4400 853 600 2060 1125 124 20.0 1 0 50 25 0.35 0.21
13 4610 4860 1380 155 12.0 0 2 80 0 0.00 0.14
I 14 5520 5410 4300 787 480 3930 1564 146 22.6 0 0 50 25 0.24 0,19
15 4100 4000 1976 159 19.5 2 50 0 0.00 0.12
16 4540 5380 5110 744 510 1410 1172 102 28.0 0 40 108 0.39 0.20
17 5230 5140 1400 139 20.0 1 50 0 0.00 0.13
I 18 4020 4930 5650 769 150 2060 1260 131 23.5 40 108 0.40 0.21
19 4180 5120 1236 134 28.5 1 1 40 0 0.00 0.16
20 3840 3930 4730 767 440 3380 1252 139 35.2 0 0 50 25 0.34 0.22
21 4530 4150 1272 141 23.2 0 0 50 0 0.00 0.15
22 4390 3770 3550 714 440 8460 1536 136 24.6 0 0 50 25 0.21 0.19
I 23 3750 3260 3090 449 560 2380 1356 121 16.1 0 1 50 81 0.20 0.15
24 3840 2980 1312 109 17.0 1 1 40 0 0.00 0.15
25 3500 2690 2500 739 500 9500 1056 165 31.0 0 0 40 25 0.21 0.12
26 4610 3210 1280 138 19.0 0 40 0 0.00 0.12
I 27 4570 3500 3720 427 140 3900 1552 148 26.6 0 0 50 25 0.21 0.13
28 4260 3340 1576 125 18.0 0 50 0 0.00 0.08
29 3960 3380 3560 380 140 11700 1420 140 23.4 0 50 25 0.22 0.13
30 3160 3590 1124 128 18.5 0 50 0 0.00 0.09
I AVG: 4436 4106 3752 627 381 5399 1360 125.5 22.9 0 1 49 33 0.15
MAX: 5580 5410 5650 853 600 11840 1976 165.0 35.2 1 2 80 108 0.40
MIN: 3160 2690 0 0 0 0 1012 89.0 12.0 0 0 40 0 0.00
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. INNER TIER COMBINED INFLUENT #2 ITCI
PAGE NO.1 I nov.2000
DATE: FLOW: PH: COD: TSS: TOC:
GPD pH ppm ppm ppm
11/01/00 1272 5.5 5020 24 1440 I
11/02/00 1399 5.6 4960 8
11/03/00 1378 5.5 4630 7 I 11/04/00 1374 5.5 4100 31
11/05/00 1364 5.4 3710 35
11/06/00 1384 5.3 5210 57
11/07/00 1433 5.5 4500 32 I 11/08/00 1330 5.5 3580 30 1360
11/09/00 1301 5.6 5060 12
11/10/00 1304. 5.6 5580 4 I 11/11/00 1352 5.6 5100 1
11/12/00 1350 5.5 5010 2
11/13/00 1440 5.4 4610 4 I 11/14/00 1397 5.5 5520 5 1640
11/15/00 1392 5.4 4100 7
11/16/00 1500 5.4 4540 4
11/17/00 1438 5.4 5230 4 I 11/18/00 1438 5.5 4020 2
11/19/00 1243 5.5 4180 4
11/20/00 1366 5.5 3840 5 I 11/21/00 1415 5.6 4530 7
11/22/00 1414 5.5 4390 10 no sample lost during transpor
11/23/00 1297 5.5 3750 6
11/24/00 1291 5.5 3840 7 I 11/25/00 1483 5.5 3500 2
11/26/00 1357 5.5 4610 4
11/27/00 1357 5.4 4570 4 I 11/28/00 1353 5.5 4260 9
11/29/00 1350 5.5 3960 4 no sample lost during transpor
11/30/00 1350 5.5 3160 6 I
AVG: 1371 5.5 4436 11 888
MAX: 1500 5.6 5580 57 1640 I MIN: 1243 5.3 3160 0
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I GROUNDWATER MONTHLY MONITORING:
INNER TIER EQUALIZATION TANK: ITEQT
I PAGE NO.2
nov.2000
DATE: PH: COD: OTWATERADDED
I
pH ppm gal
11/01/00 8.1 3210
11/02/00 8.3 3960
I 11/03/00 8.6 3990
11/04/00 8.3 4550
11/05/00 8.0 4550
I 11/06/00 8.0 4050
11/07/00 8.2 4420
11/08/00 8.0 4110
11/09/00 7.1 3440
I 11/10/00 7.6 4650
11/11/00 7.6 4770
11/12/00 7.2 4830
I 11/13/00 7.4 4860
11/14/00 7.4 5410
11/15/00 7.4 4000
I
11/16/00 7.3 5380
11/17/00 7.5 5140
11/18/00 7.5 4930
11/19/00 7.6 5120
I 11/20/00 7.4 3930
11/21/00 7.7 4150
11/22/00 7.4 3770
I 11/23/00 7.4 3260
11/24/00 7.6 2980
11/25/00 7.4 2690
11/26/00 7.6 3210
I 11/27/00 7.3 3500
11/28/00 7.6 3340
11/29/00 7.3 3380
I 11/30/00 7.6 3590
I
AVG: 7.6 4106 #DIV/0!
MAX: 8.6 5410 0
MIN: 7.1 2690 0
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GROUNDWATER MONTHLY MONITORING: I
AFTER PLATE SEPARATOR BEFORE SBR: SBRI
PAGE NO. 3 I nov.2000
DATE: PH: COD: TSS:
pH ppm ppm
11/01/00 6.5 2670 4 I
11/02/00
11/03/00 7.0 3880 8 I 11/04/00
11/05/00 5.4 3660 4
11/06/00
11/07/00 5.8 3930 68 I 11/08/00 5.9 4430 32
11/09/00
11/10/00 5.9 4660 12 I 11/11/00
11/12/00 5.6 4400 4
11/13/00 I 11/14/00 5.9 4300 8
11/15/00
11/16/00 6.9 5110 25
11/17/00 I 11/18/00 6.5 5650 20
11/19/00
11/20/00 7.1 4730 16 I 11/21/00
11/22/00 7.4 3550 36
11/23/00 7.4 3090 60
11/24/00 I 11/25/00 6.7 2500 28
11/26/00
11/27/00 7.1 3720 28 I 11/28/00
11/29/00 7.3 3560 48
11/30/00 I
AVG: 6.5 3990 25
MAX: 7.4 5650 68 I MIN: 5.4 2500 4
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50 I
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I GROUNDWATER MONTHLY MONITORING:
SBR MIXED LIQUOR: SBRML
I PAGE NO. 4
nov.2000 SETT. SLUDGE 5/DAY
DATE: PH: NH3N: PO4: DO: MLSS: MLVSS: SOLIDS: WASTED F/M: F/M:
I
pH ppm ppm ppm ppm ppm ml/I gal ratio ratio
11/01/00 8.7 145 27.5 4.9 1604 50 100 0.15
11/02/00 8.6 108 22.7 5.3 1220 50 0 0.00
I 11/03/00 8.6 91 18.3 6.0 1142 50 100 0.30
11/04/00 8.6 118 27.0 5.1 1260 50 0 0.00
11/05/00 8.6 118 27.9 4.8 1012 50 100 0.32 0.15
I 11/06/00 8.6 102 24.3 4.7 1756 50 0 0.00 0.12
11/07/00 8.6 108 22.6 5.9 1512 996 50 100 0.23 0.17
11/08/00 8.5 89 20.5 5.8 1272 50 100 0.31 0.17
11/09/00 8.6 101 29.7 2.2 1848 50 0 0.00 0.17
I 11/10/00 8.8 94 24.3 4.2 1124 50 25 0.37 0.18
11/11/00 8.8 115 16.0 5.1 1200 50 0 0.00 0.18
11/12/00 8.6 124 20.0 5.4 1125 50 25 0.35 0.21
I 11/13/00 8.6 155 12.0 4.7 1380 80 0 0.00 0.14
11/14/00 8.6 146 22.6 5.5 1564 976 50 25 0.24 0.19
11/15/00 8.6 159 19.5 4.2 1976 50 0 0.00 0.12
11/16/00 8.6 102 28.0 5.4 1172 40 108 0.39 0.20
I 11/17/00 8.5 139 20.0 5.0 1400 50 0 0.00 0.13
11/18/00 8.6 131 23.5 5.3 1260 40 108 0.40 0.21
11/19/00 8.6 167 26.5 5.1 1236 40 0 0.00 0.16
I 11/20/00 8.6 139 35.2 5.2 1252 50 25 0.34 0.22
11/21/00 8.7 141 23.2 6.2 1272 968 50 0 0.00 0.15
11/22/00 8.6 136 24.6 6.2 1536 50 25 0.21 0.19
I 11/23/00 8.5 121 16.1 5.8 1356 50 81 0.20 0.15
11/24/00 8.6 109 17.0 5.6 1312 40 0 0.00 0.15
11/25/00 8.6 165 31.0 4.2 1056 40 25 0.21 0.12
11/26/00 8.5 136 19.0 5.0 1280 40 0 0.00 0.12
I 11/27/00 8.5 148 26.6 5.5 1552 50 25 0.21 0.13
11/28/00 8.5 125 18.0 7.0 1576 1076 50 0 0.00 0.08
11/29/00 8.5 140 23.4 5.9 1420 50 25 0.22 0.13
I 11/30/00 8.5 128 18.5 5.8 1124 50 0 0.00 0.09
AVG: 8.6 127 23 5 1360 1004 49 33 0.15 0.16
I MAX: 8.8 167 35 7 1976 1076 80 108 0.40 0.22
MIN: 8.5 89 12 2 1012 968 40 0 0.00 0.08
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I 51
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GROUNDWATER MONTHLY MONITORING: I
SBR EFFLUENT:(DECANl) #4 SBRE
PAGE NO. 5 I nov.2000 WAS. NH3N PHOS.
DATE: FLOW: COD: TSS: TSS ADDED: ADDED:
GPO ppm ppm ppm gal lbs I 11/01/00 1875 603 550 10280 0 0
11/02/00 0 0 0
11/03/00 1877 618 320 11840 1 2 I 11/04/00 0 0 0
11/05/00 1918 640 540 11200 0 0
11/06/00 0 0 0 I 11/07/00 1875 651 310 2440 0 0
11/08/00 2382 692 400 1290 2
11/09/00 0 1 0
11/10/00 2567 826 400 5960 1 0 I 11/11/00 0 1 1
11/12/00 2317 853 600 2060 1 0
11/13/00 0 0 2 I 11/14/00 2271 787 480 3930 0 0
11/15/00 0 0 2
11/16/00 2082 744 510 1410 1 0
11/17/00 0 1 I 11/18/00 2163 769 150 2060 1
11/19/00 0 1 1
11/20/00 2265 767 440 3380 0 0 I 11/21/00 0 0 0
11/22/00 2430 714 440 8460 0 0
11/23/00 2420 449 560 2380 0 I 11/24/00 0 1
11/25/00 1932 739 500 9500 0 0
11/26/00 0 0 1
11/27/00 2529 427 140 3900 0 0 I 11/28/00 0 0
11/29/00 2559 380 140 11700 0
11/30/00 0 0 I
AVG: 1182 666 405 5737 0
MAX: 2567 853 600 11840 1 2 I MIN: 0 380 140 1290 0 0
* DID NOT PROCESS SBR.
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I GROUNDWATER MONTHLY MONITORIN(
INNER TIER CARBON FILTER EFFLUENT #8 ITEF
I PAGE NO. 7
nov.2000
DATE: PH: COD: TOC: TSS:
pH ppm ppm ppm
I 11/01/00 8.5 561 48 550
11/02/00
I 11/03/00
11/04/00
11/05/00
I 11/06/00
11/07/00
11/08/00 8.5 626 34
11/09/00
I 11/10/00
11/11/00
11/12/00
I 11/13/00
11/14/00 8.3 675 33
11/15/00
11/16/00
I 11/17/00
11/18/00
11/19/00
I 11/20/00
11/21/00
11/22/00 8.4 667 no sample lost during transport
I
11/23/00
11/24/00
11/25/00
11/26/00
I 11/27/00
11/28/00
11/29/00 8.3 682 no sample lost during transport
I 11/30/00
AVG: 8.4 642 23 550
I MAX: 8.5 682 48 550
MIN: 8.3 561 0 550
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I 53
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INNER TIER I DAILY FLOW
DEC. I
2000 IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9 I 12/01/00 30 19 61 84 206 0 94 403 480
12/02/00 29 13 59 83 206 0 96 371 447
12/03/00 29 20 58 91 213 0 92 395 365 I 12/04/00 29 18 59 93 219 0 86 405 244
12/05/00 29 17 60 89 204 0 84 371 232
12/06/00 29 17 60 91 200 0 94 339 231
12/07/00 29 18 59 85 204 0 93 340 224 I 12/08/00 29 17 61 95 207 0 93 354 227
12/09/00 33 16 60 89 223 0 100 353 230
12/10/00 23 16 58 89 215 0 103 372 216
12/11/00 29 17 258 82 199 0 76 384 215 I 12/12/00 29 16 60 85 189 1 81 392 206
12/13/00 27 17 0 84 185 0 102 363 184
12/14/00 28 16 0 84 186 0 84 386 191
12/15/00 28 16 3 80 186 0 89 392 193 I 12/16/00 29 17 81 88 207 0 96 433 171
12/17/00 28 16 61 94 209 2 73 32 136
12/18/00 28 17 37 107 215 0 93 285 434 I 12/19/00 51 15 52 105 223 0 99 379 564
12/20/00 50 16 40 99 224 0 98 368 547
12/21/00 50 17 45 86 231 0 109 376 563
12/22/00 51 16 43 93 230 0 107 354 576 I 12/23/00 50 15 45 90 239 0 76 312 562
12/24/00 42 17 41 95 241 0 101 265 545
12/25/00 50 15 39 94 228 0 104 236 543
12/26/00 53 16 38 90 222 0 83 232 496 I 12/27/00 56 16 38 83 237 0 103 214 518
12/28/00 55 15 41 84 236 0 108 215 505
12/29/00 54 17 41 83 238 0 107 207 504
12/30/00 54 17 40 86 225 0 112 191 530 I 12/31/00 48 16 38 83 186 0 54 192 504
AVG: 38 16 53 89 214 0 93 320 374 I
TOTAL: 1179 511 1636 2764 6633 3 2890 9911 11583
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GROUNDWATER MONTHLY MONITORING:
RAINFALL DATA
DEC 2000
DATE INCHES/DAY
12/01/00 0.00
12/02/00 0.00
12/03/00 o.oo
12/04/00 0.00
12/05/00 0.00
12/06/00 0.00
12/07/00 0.00
12/08/00 0.00
12/09/00 0.00
12/10/00 0.00
12/11/00 0.00
12/12/00 0.00
12/13/00 0.10
12/14/00 0.10
12/15/00 0.60
12/16/00 0.60
12/17/00 0.00
12/18/00 0.10
12/19/00 0.10
12/20/00 0.00
12/21/00 0.00
12/22/00 o.oo
12/23/00 o.oo
12/24/00 0.00
12/25/00 0,00
12/26/00 o.oo
12/27/00 o.oo
12/28/00 0.00
12/29/00 o.oo
12/30/00 o.oo
12/31/00 o.oo
TOTAL 1. 60
55
c..n
cr,
- -
Well
OT-2R
OT-3
OT-4
OT-5
OT-6
OT-6A
OT-7
OT-8
Thermometer
Operational? ""
X
X
X
X
X
X
X
X
Monthly O&M Plan Checklist
HNA Holdings, Inc., Shelby, NC
Heat Lamp
Operational? ""
X
X
X
X
X
X
X
X
Other Operational Items/Comments
("" Temperature and Heat Lamp checks October thru April only)
Form Completed by: __________ .:..TO=N.:..Y--'B"-R'-'Y.:..ANT=----------
Date: ___________ .:..1 ==-2'-/ 1:..,/...,0'-'0'------------- - -- - - - - - -- - - - --
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MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
ACTION
DATE WELL# PROBLEM DATE ACTION MECHANIC
12/18/00 #8 LOW FLOW 12/18/00 CHANGED METER & BLADDER
12/18/00 #9 LOW FLOW 12/18/00 CLEANED SCREEN
LU VVl''t I l"\VL~ 6.
12/19/00 #1 LOW FLOW 12/19/00 SCREEN
12/19/00 #3 LOW FLOW 12/19/00 CHANGED PUMP & CLEANED SCREEN
57
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I
DAILY REFERENCE SHEET:
DATE: IT. EQ. PLT. DEC. DEC. WAS MIX MIX MIX NIT PHOS MIX F/M I DEC. INF. TNK. SEP. LIQ LIQ LIQ ADD ADD LIQ WAS 5/DAY
2000 COD. COD. COD. COD. TSS. TSS MLSS till PHO$ GALS LBS SET. GALS F/M AVG.
1 3920 3790 3850 520 200 10720 1264 136 24.3 0 0 50 25 0.27 I 2 4210 3410 3620 549 550 2770 1344 127 15.0 0 1 50 64 0.24
3 4070 2510 2890 412 80 3480 1320 95 28.6 1 50 25 0,19
4 4090 3490 1320 85 18.5 1 2 50 0 0.00
5 4850 3800 3260 448 240 12600 1328 119 35.5 0 0 50 25 0.22 0.18 I 6 4380 4610 1368 105 22.8 0 0 50 0 0.00 0.13
7 3770 3160 3190 511 340 12260 1356 92 33.2 1 50 25 0.21 0.12
8 4500 5340 1396 118 18.6 0 0 50 0 0.00 0.09
9 4540 4040 3830 579 610 3090 1500 171 27.0 0 0 50 54 0.23 0.13
10 4870 4330 1388 110 13.1 0 1 50 0 0.00 0.09 I 11 4210 3780 4050 539 180 11560 1376 143 38.6 0 0 50 25 0.26 0.14
12 4430 3900 1252 110 26.2 0 0 50 0 0,00 0.10
13 4620 4120 4120 618 480 12080 1364 119 25.1 0 0 50 25 0.27 0.15
14 4800 3730 1364 103 15.0 0 1 50 0 0.00 0.11 I 15 4910 4360 4520 538 240 5980 1236 103 21.4 0 0 50 25 0.33 0.17
18 3850 3330 1416 104 15.0 0 50 0 0.00 0.12
17 4010 4450 4020 611 360 11900 1224 98 23.1 0 0 50 25 0.29 0.18
18 4170 3610 1338 85 16.0 1 1 50 0 0.00 0.12
19 5120 3570 4200 593 320 13400 1412 100 19.1 0 0 50 25 0.26 0.18 I 20 4150 2730 3350 618 300 14810 1248 92 13.9 50 25 0.24 0.16
21 4810 3550 8340 1288 96 18.0 1 50 25 0.00 0.16
22 4700 3330 2570 495 200 11960 1292 138 23.6 0 0 50 25 0.18 0.14
23 4740 4610 1388 109 13.0 1 1 30 0 0.00 0.14 I 24 4700 4560 3890 660 520 7620 1268 125 21.6 0 0 30 54 0.27 0.14
25 4060 4270 1280 113 13.5 1 40 0 0.00 0.09
26 4490 4050 4010 665 420 4260 1320 125 23.5 0 0 40 54 0.27 0.14
27 5220 3840 1284 104 15.8 0 0 40 0 0.00 0.11
28 3410 3400 3740 640 340 7840 1340 114 15.3 0 2 40 25 0.25 0.16 I 29 4950 3700 1436 100 20.9 0 0 40 0 0.00 0.10
30 4430 3470 3780 668 400 11740 1376 105 20.5 0 0 40 25 0.24 0.15
31 4640 4750 1360 77 16.0 40 0 0.00 0.10
AVG: 4439 3858 3699 568 340 9245 1337 110.3 21.0 0 1 46 19 0.14 I MAX: 5220 5340 4520 668 610 14810 1500 171.0 38.6 1 2 50 64 0.33
MIN: 3410 2510 2570 412 80 2770 1224 77.0 13.0 0 0 30 0 0.00
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INNER TIER COMBINED INFLUENT #2 ITCI
I PAGE N0.1
DEC.2000
DATE: FLOW: PH: COD: TSS: TOG:
GPO pH ppm ppm ppm
I 12/01/00 1377 5.5 3920 5
12/02/00 1304 5.4 4210 4
I 12/03/00 1263 5.5 4070 5
12/04/00 1153 5.5 4090 16
12/05/00 1086 5.5 4850 34 no sample lost in transport
I 12/06/00 1061 5.5 4380 42
12/07/00 1052 5.5 3770 5
12/08/00 1083 5.4 4500 5
12/09/00 1104 5.6 4540 5
I 12/10/00 1092 5.5 4870 5
12/11/00 1260 5.5 4210 4
12/12/00 1059 5.5 4430 5
I 12/13/00 962 5.5 4620 10 1500
12/14/00 975 5.5 4800 5
12/15/00 987 5.5 4910
12/16/00 1122 5.5 3850 4
I 12/17/00 651 5.5 4010 13
12/18/00 1206 5.2 4170 4
12/19/00 1488 5.5 5120 31
I 12/20/00 1442 5.2 4150 10 1370
12/21/00 1477 5.4 4810 5
12/22/00 1470 5.4 4700 4
I 12/23/00 1389 5.1 4610 7
12/24/00 1347 5.3 4700 7
12/25/00 1309 5.1 4060 11
12/26/00 1230 5.2 4490 10 1410
I 12/27/00 1265 5.4 5220 2
12/28/00 1259 5.3 3410 22
12/29/00 1251 5.3 4950 1
I 12/30/00 1255 5.1 4430 4
12/31/00 1121 5.1 4640 32
AVG: 1197 5.4 4435 10 1070
I MAX: 1488 5.6 5220 42 1500
MIN: 651 5.1 3410 0
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.1
I 59
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GROUNDWATER MONTHLY MONITORING: I
INNER TIER EQUALIZATION TANK: ITEQT
PAGE NO. 2 I DEC.2000
DATE: PH: COD: OT WATER ADDED
pH ppm gal
I 12/01/00 7.2 3790
12/02/00 7.3 3410
12/03/00 7.5 2510 563 I 12/04/00 7.6 3490
12/05/00 7.4 3800
12/06/00 7.4 4610
12/07/00 7.6 3160 75 I 12/08/00 7.4 5340
12/09/00 7.6 4040
12/10/00 7.7 4330 I 12/11/00 7.4 3780
12/12/00 7.5 3900
12/13/00 7.6 4120 188 I 12/14/00 7.6 3730
12/15/00 7.5 4360 75
12/16/00 7.7 3330
12/17/00 7.3 4450 I 12/18/00 7.5 3610
12/19/00 7.6 3570 75
12/20/00 7.5 2730 375 I 12/21/00 7.6 3550
12/22/00 7.6 3330
12/23/00 7.4 4610
12/24/00 7.4 4560 I 12/25/00 8.3 4270
12/26/00 7.4 4050
12/27/00 7.6 3840 I 12/28/00 7.5 3400
12/29/00 7.5 3700
12/30/00 7.4 3470 I 12/31/00 7.3 4750
AVG: 7.5 3858 225
MAX: 8.3 5340 563 I MIN: 7.2 2510 75
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I GROUNDWATER MONTHLY MONITORING:
AFTER PLATE SEPARATOR BEFORE SBR: SBRI
I PAGE NO. 3
DEC.2000
DATE: PH: COD: TSS:
pH ppm ppm
I 12/01/00 7.2 3850 12
12/02/00 7.4 3620 52
I 12/03/00 7.3 2890 8
12/04/00
12/05/00 7.4 3260 20
12/06/00 I 12/07/00 7.6 3190 4
12/08/00
12/09/00 7.0 3830 20
I 12/10/00
12/11/00 5.1 4050 8
12/12/00
I 12/13/00 5.6 4120 16
12/14/00
12/15/00 5.9 4520 4
12/16/00
I 12/17/00 5.9 4020 8
12/18/00
12/19/00 7.1 4200 12
I 12/20/00 7.5 3350 16
12/21/00
12/22/00 5.6 2570 4
12/23/00 I 12/24/00 6.2 3890 8
12/25/00
12/26/00 5.8 4010 16
I 12/27/00
12/28/00 5.4 3740 4
12/29/00
I 12/30/00 5.7 3780 16
12/31/00
AVG: 6.5 3699 13
I MAX: 7.6 4520 52
MIN: 5.1 2570 4
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GROUNDWATER MONTHLY MONITORING: I
SBR MIXED LIQUOR: SBRML
PAGE NO.4 I DEC.2000 SETT. SLUDGE 5/DAY
DATE: PH: NH3N: PO4: DO: MLSS: MLVSS: SOLIDS: WASTED F/M: F/M:
pH ppm ppm ppm ppm ppm ml/I gal ratio ratio I 12/01/00 8.5 136 24.3 6.3 1264 50 25 0.27
12/02/00 8.5 127 15.0 5.4 1344 50 64 0.24
12/03/00 8.5 95 28.6 5.8 1320 50 25 0.19 I 12/04/00 8.5 85 18.5 6.0 1320 50 0 0.00
12/05/00 8.5 119 35.5 6.4 1328 980 50 25 0.22 0.18
12/06/00 8.4 105 22.8 5.2 1368 50 0 0.00 0.13 I 12/07/00 8.5 92 33.2 6.3 1356 50 25 0.21 0.12
12/08/00 8.5 116 18.6 5.5 1396 50 0 0.00 0.09
12/09/00 8.6 171 27.0 5.6 1500 50 54 0.23 0.13
12/10/00 8.6 110 13.1 5.3 1388 50 0 0.00 0.09 I 12/11/00 8.5 143 38.6 6.7 1376 50 25 0.26 0.14
12/12/00 8.5 110 26.2 6.9 1252 976 50 0 0.00 0.10
12/13/00 8.5 119 25.1 7.1 1364 50 25 0.27 0.15 I 12/14/00 8.6 103 15.0 5.4 1364 50 0 0.00 0.11
12/15/00 8.5 103 21.4 6.3 1236 50 25 0.33 0.17
12/16/00 8.5 104 15.0 4.1 1416 50 0 0.00 0.12
12/17/00 8.5 98 23.1 4.4 1224 50 25 0.29 0.18 I 12/18/00 8.3 85 16.0 4.9 1338 50 0 0.00 0.12
12/19/00 8.4 100 19.1 4.1 1412 1052 50 25 0.26 0.18
12/20/00 8.3 92 13.9 4.5 1248 50 25 0.24 0.16 I 12/21/00 8.2 97 18.0 4.2 1288 50 25 0.00 0.16
12/22/00 8.3 138 23.6 4.5 1292 50 25 0.18 0.14
12/23/00 8.1 109 13.0 3.9 1388 30 0 0.00 0.14
12/24/00 8.2 125 21.6 4.2 1268 30 54 0.27 0.14 I 12/25/00 8.0 113 13.5 4.1 1280 40 0 0.00 0.09
12/26/00 8.2 125 23.5 4.0 1320 40 54 0.27 0.14
12/27/00 8.3 104 15.8 4.4 1284 1040 40 0 0.00 0.11 I 12/28/00 8.3 114 15.3 5.4 1340 40 25 0.25 0.16
12/29/00 8.3 100 20.9 4.7 1436 40 0 0.00 0.10
12/30/00 8.2 105 20.5 4.6 1376 40 25 0.24 0.15 I 12/31/00 8.1 77 16.0 4.0 1360 40 0
AVG: 8.4 110 21 5 1337 1012 46 19 0.14 0.13
MAX: 8.6 171 39 7 1500 1052 50 64 0.33 0.18 I MIN: 8.0 77 13 4 1224 976 30 0 0.00 0.09
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•• GROUNDWATER MONTHLY MONITORING:
SBR EFFLUENT:(DECANT) #4 SBRE
I PAGE NO. 5
DEC.2000 WAS. NH3N PHOS.
DATE: FLOW: COD: TSS: TSS ADDED: ADDED:
I GPD ppm ppm ppm gal lbs
12/01/00 2501 520 200 10720 0 0
12/02/00 1918 549 550 2770 0
I 12/03/00 1921 412 80 3480
12/04/00 0 1 2
12/05/00 1875 448 240 12600 0 0
I 12/06/00 0 0 0
12/07/00 1795 511 340 12260 1
12/08/00 0 0 0
12/09/00 2160 579 610 3090 0 0
I 12/10/00 0 0 1
12/11/00 1898 539 180 11560 0 0
12/12/00 0 0 0
I. 12/13/00 1974 618 480 12080 0 0
12/14/00 0 0 1
12/15/00 1913 538 240 5980 0 0
I 12/16/00 0 0 1
12/17/00 1875 611 360 11900 0 0
12/18/00 0 1
12/19/00 2111 593 320 13400 0 0
I 12/20/00 2070 618 300 14810 1 1
12/21/00 0 8340 1 1
12/22/00 2088 495 200 11960 0 0
I 12/23/00 0 1
12/24/00 2525 660 520 7620 0 0
12/25/00 0 1 1
12/26/00 2441 665 420 4260 0 0
I 12/27/00 0 0 0
12/28/00 2327 640 340 7840 0 2
12/29/00 0 0 0
I 12/30/00 2193 668 400 11740 0 0
12/31/00 0 1
I
AVG: 1148 568 340 9245 0
MAX: 2525 668 610 14810 1 2
MIN: 0 412 80 2770 0 0
• DID NOT PROCESS SBR .
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GROUNDWATER MONTHLY MONITOR IN( I
INNER TIER CARBON FILTER EFFLUENT #8 ITEF
PAGE NO. 7 I DEC.2000
DATE: PH: COD: TOC: TSS:
pH ppm ppm ppm
12/01/00 I
12/02/00
12/03/00 I 12/04/00
12/05/00 8.4 320 no sampl1 100
12/06/00
12/07/00 I 12/08/00
12/09/00
12/10/00 I 12/11/00
12/12/00
12/13/00 8.4 580 64 I 12/14/00
12/15/00
12/16/00
12/17/00 I 12/18/00
12/19/00
12/20/00 8.5 675 75 I 12/21/00
12/22/00
12/23/00
12/24/00 I 12/25/00
12/26/00 7.0 552 30
12/27/00 I 12/28/00
12/29/00
12/30/00 I 12/31/00
AVG: 8.1 532 42 100
MAX: 8.5 675 75 100 I MIN: 7.0 320 0 100
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I Attachment 2
I Analytical Data for the
July and October 2000 Sampling Events
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I Kubal-Furr & Associates
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DATA ASSESSMENT CHECKLIST REPORT -LEVEL II
Client ID:
Project Number:
Monitoring period:
CNA Holdings, Inc.-Shelby
TF026DB0I
03/00
Sample Delivery Group (SDG) Description:
Prepared By: Diane M. Rosseter
Date: 9/19/00
Quarterly monitoring well samples collected and analyzed by Davis & Floyd, Inc. of Greenwood,
SC for volatiles. semi-volatiles, ethylene glycol. and total organic carbon according to EPA
SW846 methodolo11v
CONTENTS LEVEL COMMENTS
II
Sample Results -All data Class A except as noted in
the discussion section below.
Method Conformance Summary -O.K.
Chain(s) of Custody (COCs) -Various info incomplete. No effect
on data.
Master Tracking List -O.K.
Case Narrative
Sample Prep
Standards Prep
Instrument Quality Control Data .
Batch Quality Control Report O.K. -
Surrogate Recovery Report
Trip/Field/Equipment Blank Report -O.K.
Field Notes/Logbook -Various info incomplete. No effect
on data.
CLP Forms
All Raw Data
Electronic Deliverables -O.K.
Discussion:
I. Results for ethylene glycol exceeded the calibration range during the initial analysis of sample
ITC!. The sample was diluted and reanalyzed out of holding time. Results from both
analytical runs were reported by the laboratory and qualified as estimated. These results were
flagged with "J".
Kubal-Furr & Associates
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J = positively identified, however concentration is estimated
Class A= quantitative Class B = qualitative
Kubal-Furr & Associates
Class C = unusable
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.l)C..,._,; ()",(_"'-' ~ -V V 7:.,
DAYIS
FLtJ\1D LABORATORY ANALYSIS REPORT
September 19, 2000
JERRY MCMURRAY
HNA HOLDINGS INC.
PO BOX 87
SHELBY, NC 28150
Login Number
Project Number
Description
:100072001
:61195.00-0003
:PLANT SITE WELLS -REVISED 19-SEP-00
Dear Jerry Mcmurray:
We are pleased to provide the enclosed analytical results for the samples received by
Davis & Floyd, Inc. on July 20, 2000.
A formal Quality Assurance/Quality Control program is maintained by Davis & Floyd,
which is designed to meet or exceed the EPA or appropriate regulatory requirements.
All analytical analyses for this project met QA/QC criteria unless otherwise stated in the
footnotes. This report is to be reproduced only in full.
Feel free to contact our Client Services Representative at [phone] if further
explanation of the analysis is required. Unless other arrangements have been made, samples
will be disposed of or returned 14 days from the date of the report. We appreciate the
opportunity to provide services to your firm.
Sincerely,
DA
0
~:S & JOY/ INC.
1.#>I
hn H. McCord, Jr.
aboratory Manager
I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I {864) 229-4413 I Fax {864) 229-7119
1
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Method Conformance Summary
Client Ticona, LLC
Login(s): L00072001
Critetria Volatiles
Sample Holding Time
Standards Preparation
Instrument Tuning
Instrument Calibration
Calibration Verification
Degradation Check
Interference
Sample/Standard
Blanks Results
Method Accuracy
Method Precision
Surrogate Recovery
PDSISDIMSA
TCLP Preparation
Key ✓
NIA
= Met Criteria Met
= Not Applicable
v
v v v v
NIA
NIA
v
v
v
•
NIA
NIA
Semi
Volatiles
v v v v
v
NIA
NIA
v
v
• v
NIA
NIA
Metals
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
•
PDS =
SD =
MSA=
Method Criteria Not Met -See footnote(s) below .
Post Digestion Spike
Serial Dilution
Method of Standard Additions
Project Number: 61995.00-0003
Report Date: August 15, 2000
Inorganics Other
v v
v v
NIA NIA
v v
✓ v
NIA NIA
NIA NIA
v v v v
v v
NIA NIA
NIA NIA
NIA NIA
Footnotes: TOC analyses summarized under column headed "Inorganics".
Ethylene glycol summarized under column headed "Other".
Volatiles -The surrogate 1,2-dichloroethene recovered high in the MS and MSD
{125.6% and I25.7% respectively). The upper control range is 122%.
Semivolatiles -The RPD for pentachlorophenol was 28.3%. The RPD limit is 28%.
Ethylene glycol was initially analyzed on 7126100 within holding time. Sample
L00072002-03 (ITC!) exceeded the calibration range. The sample was diluted
analyzed successfully on 7131100.
Preparedb>(Ji ~(__
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Davis & Floyd, Inc. I PO D,awe, 428 I G,eenwood, SC 29648 I 816 E. ~ucst Avenue I G,eenwood, SC 29649 I [phone] I fax [phone]
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Di\YIS
FLt1YD LABORATORY ANALYSIS REPORT
Master Tracking List
Sample ID
L000i2001-0l
Field Data
EPA 170.l
SW846 904 OB
SW846 9050
Client
Contact
Volatile Organics
SW846 8260B
L00072001-02
Field Data
EPA 170.1
SW846 9040B
SW846 9050
Gas Chromatography
SW846 8015
Volatile Organics
SW846 8260B
Wet Chemistry
SW846 9060
L0007200l-03
Field Data
EPA 170.
SW846 9040B
SW846 9050
Gas Chromatography
SWB46 8015
Volatile Organics
SW846 826GB
Wet Chemistry
SW846 9060
HNA HOLDINGS INC.
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID
CC-33
ITEF
ITCI
Project Number: 61195.00-0003
Report Date
Page 1 of 7
September 05, 2000
Date Collected
19-JUL-00 09:14
Date Received
07/19/00 0914
07/19/00 0914
07/19/00 0914
07/20/00 1302
19-JUL-00 09:31 20-JUL-00
19-JUL-00 09:43
07/19/00 0931
07/19/00 0931
07/19/00 0931
07/26/00 0329
07/20/00 1326
07/27/00 0940
20-JUL-00
07/19/00 0943
07/19/00 0943
07/19/00 0943
07/26/00 0358
07/20/00 2104
07/27/00 1140
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 1 [phone] I Fax [phone]
3
DAYIS
FLtJ\1D LABORATORY ANALYSIS REPORT
Master Tracking List
Sample ID
L00072001-04
Field Data
EPA 170.l
SW846 9040B
SWB46 9050
Client
Co11tact
Semivolatile Organics
SW846 8270C
$W846 8270C DOWTHER.M
Volatile Organics
SW846 826GB
L00072001-0S
Field Data
EPA 170.1
SW846 904GB
SWB46 9050
Semivolatile Organico
SW846 8270C
SW846 8270C DOl,<lTHERM
Volatile organico
SW846 8260B
L00072001-06
Field Data
EPA 170.l
SW846 9040B
SW846 9050
Semivolatile Organics
sws,16 s21oc
SW846 8270C DOWTHERM
Volatile Organics
SW846 8260B
HNA HOLDINGS INC.
PO BOX 87
GHELBY, NC 28150
JERRY MCMURRAY
Client ID
PEW-1
PEW-3
PEW-3 DUP.
Project Number: 61195.00-0003
Report
Page 2
Date Collected
19-JUL-OO
07/20/00 1145
07/20/00 1145
19-JUL-OO
07 /20/00 1145
07/20/00 1145
07 /20/00 1145
07/20/00 1145
10: 52
11:28
Date Auguot 15, 2000
of 7
Date Received
20-JUL-00
07/19/00 1052
07/19/00 1052
07/19/00 1052
07/27/00 1735
07/27/00 1735
07/20/00 1414
20-JUL-OO
07/19/00 1128
07/19/00 1128
07/19/00 1128
07/27/00 1926
01 /21 /oo 1926
07/20/00 1439
20-JUL-OO
07/19/00 112 B
07/19/00 1128
07/19/00 1128
07/27/00 2003
07 /27 /00 2003
07/20/00 1503
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Davis & Floyd, Inc. j PO Drawer 428 I Greenwood, SC 29648 l 816 E. Ours! Avenue
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I Greenwood, SC 29649 I (864i 229-4413 I fax [phone]
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DAYIS
FLtJ\1D LABORATORY ANALYSIS REPORT
Master Tracking List
Sample ID
L00072001-07
Field Data
EPA 170.l
SW846 9040B
SW846 9050
r:1 -i.ent
Canta.ct
Semivolatile Organics
SW846 8270C
SW846 8270C DOWTHERM
Volatile Organics
SW846 8260B
L00072001-08
Field Data
EP.:\ 170.
SW846 9040B
SW846 ;}050
Semivolatile organics
SWB46 B270C
SW846 8270C DOWTHERM
Volatile Organics
SW846 8260B
L00072001-09
Field Data
EPA 170.
SW846 9040B
SW846 9050
Volatile Organics
SW846 8260B
HNA HOLDINGS INC.
E-'O BOX 87
.SHELBY, NC 28150
JERRY MCMURRAY
client IO
PEW-4
P-58
07 /20/00
07/20/00
07 /20/00
07/20/00
Project Number: 61195.00-0003
Report Date
Page 3 of 7
Diil.te Collected
19-JUL-00 12:00
07/19/00
07/19/0D
01/19/oo
1145 07/27/00
1145 07/27/00
07/20/00
H-JUL-00 11:50
07/19/oo
07/19/00
07/19/oo
1145 07/27/00
1145 o7/2S/oo
07/20/00
19-JUL-00 13:20
07/19/00
07/19/00
07/19/00
Auguot 15, 2000
Date Received
20-JUL-00
1200
1200
1200
2 04 0
2040
152 7
2D-JUL-00
1150
11-50
1150
2117
1202
1552
20-JUL-OO
1320
1320
1320
07/20/00 1616
Davis & Floyd, Inc. I PO Drawer 428 ! Greenwood, SC 29648 I 816 E. 5urst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLtJ\'D LABORATORY ANALYSIS REPORT
Master Tracking List
Slll!lple ID
L00072001-10
Field Data
EPA 170.1
SW846 9040B
SW846 9050
client
Cont<•ct
Volatile Organics
SW846 8260B
L00072001-ll
Field Data
Ep_:i 170.1
SW8.J6 90.J0B
SW846 9050
Volatile Organics
SW846 8260B
L00072001-12
Field Data
EP.J. 170.1
SW846 904GB
SW846 9050
Volatile Organics
SW84 6 826GB
L00072001-13
Field Data
EPil 170.1
SW846 904GB
SW846 9050
Volatile Organics
SW846 82i>OB
HNA HOLDINGS INC.
PO BOX 87
r;HELBY, NC 28150
JERRY MCMURRAY
client ID
EE-58
C-49
HH-77
HH-48
Project Number: 61195.00-0003
Report Date
Page 4 of 7
Dato Collected
19-JUL-OO 14: 07
07/19/00
07/19/00
07/19/00
07/20/00
19-JUL-00 15:36
07/19/00
07/19/00
07/19/00
07/20/00
19-JUL-OO 16: 32
07/19/00
07/19/00
07/19/00
07/20/00
19-JUL-OO 16:35
07/19/00
07/19/00
07/19/00
Augu:lt 15, 2000
Date Received
20-JUL-OO
1407
1407
1407
1640
20-JUL-00
1536
1536
1536
1752
20-JUL-OO
1632
1532
1632
1816
20-JUL-OO
1635
163 5
1635
07/20/00 1840
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Davis & Floyd, Inc. \ PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue
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I Greenwood, SC 29649 I [phone] I Fax [phone]
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Di\YIS
FLOYD LABORATORY ANALYSIS REPORT
Master Tracking List
Sample ID
Field Data
EPA 170.
SW846 9040B
SWB46 9050
client
Cont.act
Volatile Organics
SW846 B26·os
L00072001-15
Field Data
EP . ."\. 17n
SW846 90't0E
SW846 9050
Volatile Organics
SW846 8260E
L00072001-16
Field Data
EP . ."\. 170.1
SW846 9040B
SW846 9050
Volatile Organics
SW846 82608
L00072001-17
Field Data
EPA 170.1
Sf'1846 9040B
SW846 9050
Volatile Org,mics
SW846 8260E
HNA HOLDINGS INC.
!:'0 BOX 87
:,HBLBY, NC 281S0
,TERRY MCMURRAY
client ID
T-35
FF-34
GG-61
Project Number: 61195.00-0003
Report Date Auguct 15, 2000
Page 5 of 7
o .. t. Collected Date Received
19-JUL-OO 17:30 20-JUL-OO
01/19/oo 1730
01/u/oo 1730
07/19/00 1730
01/20/00 1904
19-JUL-OO 18:25 20-JUL-OO
07/l';J/OO 1825
07/19/00 1825
07/19/00 1825
07/20/00 1928
19-JUL-OO 18:35 20-JUL-00
07/19/oo 1835
07/19/00 1835
07/19/00 1835
01/20/00 1952
U-JUL-00 19:35 20-JUL-00
07/19/oo 1935
07 /B/00 1935
07/19/00 193 5
07/20/00 2016
Davis & Floyd, Inc. I PO Drawer 428 \ Greenwood, SC 29648 I 816 E. Durst Avenue
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I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLt1YD LABORATORY ANALYSIS REPORT
Master Tracking List
Sample ID
L00072001-18
Field Data
EPA 170.
SW846 9040E
SW846 9050
r:l ient
Contact
Volatile Organico
SW846 8260B
L00072001-19
Field Data
EPl!. 170.1
SWB46 9040B
SW846 9050
Volatile Organics
SW846 8260B
L00072001-20
Field Data
EPA 170.1
SW846 9040B
SW846 9050
Volatile Organics
SW846 82608
Wet Chemistry
SW846 9060
L00072001-21
Field Data
EP.;J. 170.1
SW846 9040B
SW846 9050
HNA HOLDINGS INC.
PO BOX 87
;;HELBY, NC 28150
JERRY MCMURRAY
Client ID
GG-61 DUP.
AA-54
K-28
V-23
Project Number: 61195.00-0003
Report
Page 6
Date Collected
19-JUL-OO 19:35
19-JUL-00 20:08
Date Augu!lt 15, 2000
of 7
Date Received
20-JUL-OO
07/19/00 1935
07/19/00 1935
07/19/00 1935
01/20/00 2040
20-JUL-00
07/19/00 2008
07/19/00 2008
07/19/00 2008
07/21/00 0918
19-JUL-00 20:20 20-JUL-OO
07/19/00 2020
07/19/00 2020
07/19/00 2020
07/21/00 1030
07/27/00 1330
19-JTJL-00 20:45 20-JUL-00
07/19/00 2045
07/19/00 2045
07/19/00 2045
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. gurst Avenue I Greenwood, SC 29649 I [phone] I Fax {B64) 229-71191
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DAYIS
FLtJ\1D LABORATORY ANALYSIS REPORT
Master Tracking List
,:1 ient
Cont:£ict
Sample ID
Volatile Organics
SW846 ti260E
Wet Chemistry
SW846 9060
L00072001-22
Volatile Organics
SW846 82G0E
L00072001-23
Volatile Organics
SW846 .'126"05
HNA HOLDINGS INC.
PO BOX 87
.':HEI.BY, NC 28150
,JERRY MCMURRAY
Client ID
FIELD BLANK
TRIP BLANK
Project Number: 61195.00-0003
Report Date
Page 7 of 7
Augu!Jt 15, 2000
Date Collected Date Received
01/21/00 1657
01/21/00 1421
19-JUL-OO 20:50 2O-JUL-OO
01/20/00 1230
18-JUL-OO 17:05 20-JUL-OO
07/20/00 1214
Davis & Floyd, Inc. l PO Drawer 428 I Greenwood, SC 29648 ! 816 E. Durst Avenue I Greenwood, SC 29649 l (864). 229-4413 I Fax [phone]
9
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Di\VIS
FLOYD LABORATORY ANALYSIS REPORT I
Client
Contact
RNA HOLDINGS INC.
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: CC-33
Paramoter
Field Data
EPA 170."l
TEMPERATURE
SW846 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1, 1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL 2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
GW/ChemW
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Result
18.0
,.o
295
788.24
0.0050
0.0050
0 .0050
0 . 0050
o. 0050
0. 0050
0.0050
0. 010
o. 010
0.0050
0.010
0.0050
0.0050
0.0050
0.010
o. 0050
0. 0050
0 .0050
0.010
0. 0050
0.010
0 .0050
o. 0050
o. 0050
0. 0050
0 .0050
0.0050
0.0050
o.ooso
0.0050
Davis & Floyd, Inc. \ PO Drawer 428 ( Greenwood, SC 29648 I 816 E. Durst Avenue
1 0
Project Number: 61195.00-0003
Report Date
Page 1 of 2
Sample ID
September 19, 2000
L00072001-01
Date Collected: 19-JUL-OO 09: 14
Date Received 20-JUL-OO
Qual RDL Units Analyst Date Time
1.0 degrees C 07/19/00 0914
0.50 SU 07/19/00 0914
1.0 umhos/cm 07/19/00 0914
.01 feet MSL 07/19/00 0914
0.0050 mg/1 PAP 07/20/00 1302
o. 0050 mg/1 PAP 07/20/00 1302
0 . 0050 mg/1 PAP 07/20/00 1302
0 . 0050 mg/1 PAP 07/20/00 1302
0. 0050 mg/1 PAP 07/20/00 1302
0 . 0050 mg/1 PAP 07/20/00 1302
0.0050 mg/1 PAP 07/20/00 1302
0.010 mg/1 PAP 07/20/00 13 02
0.010 mg/1 PAP 07/20/00 1302
0.0050 mg/1 PAP 07/20/00 1302
0. 010 mg/1 PAP 07 /20/00 1302
0.0050 mg/1 PAP 07/20/00 1302
0.0050 mg/1 PAP 07/20/00 1302
0.0050 mg/1 PAP 07/20/00 1302
0.010 mg/1 PAP 07/20/00 1302
0.0050 mg/1 PAP 07/20/00 1302
0.0050 mg/1 PAP 07/20/00 1302
0.0050 mg/1 PAP 07/20/00 1302
0.010 mg/1 PAP 07/20/00 13 02
0.0050 mg/1 PAP 07/20/00 13 02
0. 010 mg/1 PAP 07/20/00 1302
0.0050 mg/1 PAP 07/20/00 1302
0.0050 mg/1 PAP 07/20/00 1302
0 .0050 mg/1 PAP 07/20/00 1302
o. 0050 mg/1 PAP 07/20/00 1302
0.0050 mg/1 PAP 07/20/00 1302
o.ooso mg/1 PAP 07/20/00 1302
0 .0050 mg/1 PAP 07/20/00 1302
0 .0050 mg/1 PAP 07/20/00 1302
0 . 0050 mg/1 PAP 07/20/00 1302
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DAYIS
FLtfvD LABORATORY ANALYSIS REPORT
Client HNA HOLDINGS INC. Project Number: 61195. 00-0003
PO BOX 87
SHELBY, NC 28150 Report Date September 19, 2000
Contact JERRY MCMURRAY Page 2 of 2
Client ID: CC-33 sample ID L00072001-0l
Para.meter Result Qual RDL Units Analyst Date Time
TRANS-1,3-DICHLOROPROPENE < 0.0050 0 .0050 mg/1 PAP 07/20/00 1302
TRICHLOROETHENE 0,0059 0 0050 mg/1 PAP 07/20/00 1302
VINYL ACETATE < 0. 010 0.010 mg/1 PAP 07/20/00 1302
VINYL CHLORIDE < 0.010 0.010 mg/1 PAP 07/20/00 1302
XYLENE (TOTAL) < o.ooso 0.0050 mg/1 PAP 07/20/00 1302
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue \ Greenwood, SC 29649 \ (864) 229-441 3 \ Fax [phone]
1 1
DAYIS
FLtJ¥D LABORATORY ANALYSIS REPORT
Client
Contact
RNA HOLDINGS INC.
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITEF
Parameter
Field Data
EPA 170, l
TEMPERATURE
SW846 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Gas Chromatography
SW846 8015
ETHYLENE GLYCOL
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE·
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-l,2·0ICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
GW/Chemw
'
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'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
' <
'
Result
27.0
8.6
3700
NA
7.0
0. 0050
0 .0050
0.0050
0 .0050
0. 0050
0. 0050
0 .0050
0. 010
0.010
0.0050
0.010
0 .0050
0 .0050
o. 0050
0. 010
0.0050
0.0050
0.0050
0. 010
0.0050
0. 010
0. 0050
0 .0050
0 .0050
o. 0050
0 . 0050
Project Number: 61195.00-0003
Report Date
Page 1 oE 2
Sample ID
September OS, 2000
L00072001-02
Date Collected: 19-JUL-OO 09:31
Date Received 20-JUL-00
Qual RDL Units Analyst Date Time
1.0 degrees C 07/19/00 0931
a.so SU 07/19/00 0931
1.0 umhos/cm 07/19/00 0931
. 01 feet MSL 07/19/00 0931
7.0 mg/1 JMT 07/26/00 0329
o. 0050 mg/1 PAP 07/20/00 1326
0 .0050 mg/1 PAP 0?/20/00 1326
0. 0050 mg/1 PAP 07/20/00 1326
0 .0050 mg/1 PAP 07/20/00 1326
0 .0050 mg/1 PAP 07/20/00 1326
o. 0050 mg/1 PAP 07/20/00 1326
0 .0050 mg/1 PAP 07/20/00 1326
0. 010 mg/1 PAP 07/20/00 1326
0.010 mg/1 PAP 07/20/00 1326
0.0050 mg/1 PAP 07/20/00 1326
0.010 rng/1 PAP 07/20/00 1326
0 .0050 mg/1 PAP 07/20/00 1326
0 . 0050 mg/1 PAP 07/20/00 1326
0 .0050 rng/1 PAP 07/20/00 1326
0. 010 mg/1 PAP 07/20/00 1326
0.0050 rng/1 PAP 07 /20/00 1326
0.0050 mg/1 PAP 07/20/00 1326
0.0050 rng/1 PAP 07/20/00 1326
0.010 mg/1 PAP 07/20/00 1326
0.0050 rng/1 PAP 07/20/00 1326
0. 010 rng/1 PAP 07/20/00 1326
0.0050 mg/1 PAP 07/20/00 1326
0.0050 rng/1 PAP 07/20/00 1326
o. 0050 mg/1 PAP 07/20/00 1326
0 .0050 mg/1 PAP 07/20/00 1326
0 .0050 mg/1 PAP 07/20/00 1326
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Davis & Floyd, Inc. I PO Dcawer 428 I Greenwood, SC 29648 I 816 Ei 2urst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC,
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITEF
Parameter
STYRENE
TETRACHLQROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Wet Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
Result
' 0 .0050
' 0 .0050
' 0 . 0050
' 0 .0050
' 0 .0050
' 0 .0050
' o. 010
' 0 .010
' 0.0050
12.0
Project Number: 61195. 00-0003
Report Date September 05, 2000
Page 2 of 2
Sample ID L00072001-02
Qual RDL Units Analyst Date Time
0 .0050 mg/1 PAP 07/20/00 1326
0. 0050 mg/1 PAP 07/20/00 1326
0 . 0050 mg/1 PAP 07/20/00 1326
0.0050 mg/1 PAP 07/20/00 1326
0 .0050 mg/1 PAP 07/20/00 1326
0 .0050 mg/1 PAP 07/20/00 1326
o. 010 mg/1 PAP 07/20/00 1326
0 .010 mg/1 PAP 07/20/00 1326
0.0050 mg/1 PAP 07/20/00 1326
1.0 TRB 07/27/00 0940
Davis & Floyd, lnc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue ! Greenwood, SC 29649 I [phone] I Fax [phone]
13
DAYIS
FLclYD LABORATORY ANALYSIS REPORT
Client
Contact
Irn'A HOLDINGS INC.
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITCI
Parameter
Field Data
EPA 170.'l
TEMPERATURE
SW846 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Gas Chromatography
SWB46 8015
ETHYLENE GLYCOL
ETHYLENE GLYCOL
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLQROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOOICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
OlLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
GW/ChemW
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
Result
27.0
5.2
2000
NA
"' 802
0. 0050
0. 0050
0.0050
0. 0050
0 . 0050
0 .0050
0. 0050
0. 010
0.010
0.0050
0.13
0.029
0.0050
0.0050
0.010
0.0052
0.0050
0.020
0.010
0.0050
0.010
0.0050
0. 0050
o. 0050
0 . 0050
Project Number: 61195.00-0003
Report Date
Page l of 2
Sample ID
Date Collected:
Date Received
Qual
..
RDL
l.O
a.so
l.O
.01
7.0
70.0
0.0050
o. 0050
o. 0050
0 .0050
o. 0050
0.0050
0.0050
0.010
0.010
0.0050
0.010
0 .0050
o. 0050
0 .0050
0.010
0 .0050
0. 0050
0 .0050
0.010
0.0050
0.010
o. 0050
0 . 0050
o. 0050
0. oosci
September 05, 2000
L00072001-03
19-JUL-00 09 : 43
20-JUL-00
Units Analyst Date Time
degrees C
SU
umhos/cm
feet MSL
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
07/19/00 094)
07/19/00 094)
07/19/00 0943
07/19/00 0943
JMT 07/26/00 0358
JMT 07/31/00 2129
PAI_> 07/20/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
PAP 07 /20/00 2104
PAP 07/20/00 2104
PAP 07 /2 0/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
PAP 07/20/00 2104
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Davis & Floyd, Inc. I PO Drnwe, 428 I G,eenwood, SC 29648 I 816 E.{r'' Avenue I G,eenwood, SC 29649 I [phone] I fax [phone] I
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DAYIS
FLtiYD LABORATORY ANALYSIS REPORT
Client HNA HOLDINGS INC.
PO BOX 87
Project Number:
Contact
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITCI
Parameter
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Wet Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
Sample comments: Ethylene Glycol
Report
Page 2
Sample
Result Qual
< o. 0050
' 0 .ooso
< 0 .0050
' 0 . 0050
0 .0050
' o.ooso
' 0.0050
< 0.010
' 0.010
' 0.0050
1580
* Sample concentration exceeded the calibration range.
The result is estimated.
Date
of 2
ID
RDL
0. 0050
0 .0050
0 . 0050
0 .0050
0 .0050
o. 0050
0 .0050
o. 010
0 .010
0.0050
10.0
** Due to instrument problems the reanalysis of the diluted
sample was analyzed out of the seven day hold time .. The
result reported should be considered as estimated.
61195.00-0003
September 05, 2000
L00072001-03
units Analyst Date Time
mg/1 PAP 07/20/00 2104
mg/1 PAP 07/20/00 2104
mg/1 PAP 07/20/00 2104
mg/1 PAP 07/20/00 2104
mg/1 PAP 07/20/00 2104
mg/1 PAP 07/20/00 2104
mg/1 PAP 07/20/00 2104
mg/1 PAP 07/20/00 2104
mg/1 PAP 07/20/00 2104
mg/1 PAP 07/20/00 2104
mg/1 TRB 07/27/00 1140
Davis & Floyd, Inc. I PO Drawer 428 \ Greenwood, SC 29646 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
15
DAYIS
FLt1YD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC,
PO BOX B7
SHELBY, NC 26150
JERRY MCMURRAY
Client IO: PEW-1
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
SWB46 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Semivolatile Organics
SW846 8270C
1,2,4-TRICHLOROBENZENE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4,S-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DICHLOROPHENOL
GW/ChemW
2, 4-DIMETHYLP!IENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENB
2-CHLORONAf'HTHALBNE
2-CHLOROPHENOL
2-MBTHYL-4,6-0INITROPHENOL
2-METHYLNAPHTHALBNE
2-METHYLPHENOL
2-NITROANILINE
2-NITROPHENOL
3,3'-DICHLOROBENZIDINB
3-NITROANILINE
4-BROMOPHENYL PHENYL ETHER
4-CHLOR0-3-M&THYLPHENOL
4-CHLOROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-METHYLPHBNOL
4-NITROANILINE
4-NITROPHENOL
ACENAPHTHENE
ACENAPHTHYLBNE
ANTHRACBNB
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I
I
Project Number: 61195. 00-0003
Report Date Augu::;t 15, 2000
Page l of 4
Sample ID L00072001-04
Date Collected: 19-JUL-OO 10 : 52 I
Date Received 20-JUL-OO
Result Qual RDL Units Analyst Date Time I
20.0 1. 0 degree!! C 07/19/00 1052 I
5,4 0.50
46,0 l. 0 umhos/cm
OU 07/19/00 1052
07/19/00 1052 I
BOO. 77 .01 feet MSL 07/19/00 1052 I
' 0.010 0.010 mg/1 JRN 07/27/00 1735
' 0. 010 0 .010 mg/1 JRN 07/27/00 1735 I
' 0. 010 0.010 mg/1 JRN 07 /27 /oo 1735
' 0.010 0.010 mg/1 JRN 07/27/00 1735
' 0.010 0. 010 mg/1 JRN 07/27/00 1735
' 0 .010 0. 010 mg/1 JRN 07/27/00 1735 I
' 0. 010 o. 010 mg/1 JRN 07/27/00 1735
' 0 .010 0.010 mg/1 JRN 07/27/00 1735
' 0.025 0. 025 mg/1 JRN 07/27/00 1735
' 0.010 0.010 mg/1 JRN 07/27/00 1735 I
' 0. 010 0 .010 mg/1 JRN 07/27/00 1735
' 0 .010 0 . 010 mg/1 JRN 07/27/00 1735
' o. 010 0.010 mg/1 JRN 07/27/00 1735 I
' 0.025 0. 025 mg/1 JRN 07/27/00 1735
' 0. 010 o. 010 mg/1 JRN 07/27/00 1735
' 0 .010 0.010 mg/1 JRN 07/27/00 1735
' 0.010 0. 010 mg/1 JRN 07/27/00 1735 I
' 0. 010 0.010 mg/1 JRN 07/27/00 1735
' 0.010 0.010 mg/1 JRN 07/27/00 1735
' 0 .010 0.010 mg/1 JRN 07/27/00 1735
' 0.010 0.010 mg/1 JRN 07/27/00 1735 I
' 0 .010 0.010 mg/1 JRN 07/27/00 1735
' 0 .010 0.010 mg/1 JRN 07/27/00 1735
' 0.010 0.010 mg/1 JRN 07/27/00 1735
' 0.010 0 .010 mg/1 JRN 07/27/00 1735 I
' 0 .010 0.010 mg/1 JRN 07/27/00 1735
' 0 . 025 0.025 mg/1 JRN 07/27/00 1735
' 0. 010 0 .010 mg/1 JRN 07/27/00 1735
' 0 .010 0 .010 mg/1 JRN 07/27/00 1735
' 0.010 0 .010 mg/1 JRN 07/27/00 1735 I
816 E. Durst Avenue
16
I Greenwood, SC 29649 I [phone] I Fax [phone]
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Df\YIS
FLOYD LABORATORY ANALYSIS REPORT
Client HNA. HOLDINGS INC. Project Number: 61195.00-0003
PO BOX 87
.',!-!ELBY, NC 28150 Report Date Augu□t 15, 2000
Contact JERRY MCMURRAY Page 2 of '
Client ID: PEW-1 Sample ID L0007200l-04
Parameter Raault Qua.l RDL Unite Analy11t Date Time
BENZO(A)ANTHRACENE < 0 .010 0.010 mg/1 JRN D7/27/00 1735
BENZO (A) PYRENE < 0.010 0. 010 mg/1 JRN 07/27/00 1735
BENZO(B)FL\JORANTHENE < 0.010 0 . 010 mg/1 JRN 07/27/00 1735
BENZO (G, H, I} f'EP.YLENE < 0.010 o. 010 mg/1 JRN 07/27/00 1735
BENZO(K)FLUORANTHENE < 0.010 0. 010 mg/1 JRN 07/27/00 1735
BENZOIC ACID < 0 . 050 0 . 050 mg/1 JRN 07/27/00 1735
BENZYL ALCOHOL < 0, 010 0.010 mg/1 JRN 07/27/00 1735
BIS(2-CHLOROETHOXY)METHANE < 0.010 0. 010 mg /1 JRN 07/27/00 1735
BIS(2-CHLOROETHYL)ETHER < 0, 010 0.010 mg/1 JRN 07/27/00 1735
BIS(2-CHLOROISOPROPYL)ETHER < 0 .010 0. 010 mg/1 JRN 07/27/00 1735
BIS(2-ETHYLHEXYL)PHTHALATE < 0.010 0.010 mg/1 JRN 07 /27 /00 1735
BUTYL BENZYL PHTHALATE < 0.010 0.010 mg/1 JRN 07/27/00 1735
CHRYSENE < 0. 010 0.010 mg/1 JRN 07/27/00 1735
Dl-N-BUTYL PHTHALi\.TE ' 0.010 0.010 mg/1 JRN 07/27/00 1735
DI-N-OCTYL PHTHALATE 0, 010 0.010 mg/1 JRN 07/27/00 1735
DIBENZ(A,H)ANTHRACENE 0 . 010 0 . 010 mg/1 JRN 07/27/00 1735
DIBENZOFURAN < 0, 010 0 .010 mg/1 JRN 07/27/00 1735
DIETHYL PHTHALATE < 0 .010 0. 010 mg/1 JRN 07/27/00 1735
DIMBTHYL PHTHALATE < 0.010 0 .010 mg/1 JRN 07/27/00 1735
FLUORANTHENE < 0 .010 o. 010 mg/1 JRN 07 /27 /00 1735
FLUORENE < 0. 010 0.010 mg/1 JRN 07/27/00 1735
HEXACHLOROBENZENE < 0.010 0 .010 mg/1 JRN 07/27/00 1 73 5
HEXACHLOROBUTADIENE ' 0,010 0.010 mg/1 JRN 07/27/00 1735
HEXACHLOROCYCLOPENTADIENE ' 0, 010 0. 010 mg/1 JRN 07/27/00 1735
HEXACHLOROETHANB < 0.010 0.010 mg/1 JRN 07/27/00 1735
INDENO(l,2,3-CD)PYRENE < 0 .010 0 .010 mg/1 JRN 07/27/00 1735
ISOPHORONE < 0. 010 0 .010 mg/1 JRN 07/27/00 1735
N-NITROSODI-N-PROPYLAMINE ' 0 .010 0 .010 mg/1 JRN 07 /27 /O? 1735
N-NITROSOOI PHENYLAM INE ' 0 .010 0.010 mg/1 JRN 07/27/00 1735
NAPHTHALENE < 0.010 0.010 mg/1 JRN 07/27/00 1735
NJ.TROBENZENE < 0 .010 o. 010 mg/1 JRN 07/27/00 1735
PENTACHLOROPHENOL < 0.025 0.025 mg/1 JRN 07/27/00 1735
PHENANTHRBNE < 0 .010 0. 010 mg/1 JRN 07/27/00 1735
PHENOL < 0.010 0 .010 mg/1 JRN 07/27/00 1735
PYRENE < 0 .010 0.010 mg/1 JRN 07/27/00 1735
SW846 B270C: DOWTHER!-1
1,1'-BIPHBNYL < 0.010 0.010 mg/1 JRN 07/27/00 1735
BIPHENYL ETHER < 0 .010 0.010 mg/1 JRN 07/27/00 1735
Davis & Floyd, lnc. I PO Drawer 428 l Greenwood, SC 29648 j 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-441 3 I fax [phone]
1 7
I
n~s LABORATORY ANALYSIS REPORT FL D
I
I
Client HNA HOLDnms INC. Project Number; 61195.00-0003
PO BOX 87
.SHELBY, NC 281S0 Report Date Auguct 15, 2000 I
Cont.act JERRY MCMURRAY Page 3 of 4
Client ID: PEW-1 Sample ID L00072001-04 I
Parameter Result Qual RDL units Analyst Date Time
Volatile Organics I SW846 8260B
1, 1, 1-TRICHLOROBTHANE < 0 .0050 0.0050 mg/1 PAP 07/20/00 1414
1,1,2,2-TETRACHLOROETHANE < 0 .0050 0 .0050 mg/1 PAP 07 /20/00 1414
1,1,2-TRICHLOROETHANE < 0 .0050 0.0050 mg/1 PAP 07/20/00 1414
1,1-DICHLOROETHANE < 0.0050 0.0050 mg/1 PAP 07/20/00 1414 I
1,1-DICHLOROETHENE < 0.0050 0 .0050 mg/1 PAP 07/20/00 1414
1,2-DICllLOROETHANE < 0.0050 0.0050 mg/1 PAP 07/20/00 1414
1,2-DICHLOROPROPANE < 0.0050 0.0050 mg/1 PAP 07/20/00 1414 I
2-BUTANONE < 0 .010 0 .010 mg/1 PAP 07/20/00 1414
2-HEXANONE < 0 .010 o·. 010 mg/1 PAP 07/20/00 1414
4-METHYL-2-PENTANONE < 0.0050 0.0050 mg/1 PAP 07/20/00 1414
ACETONE < 0.010 0.010 mg/1 PAP 07/20/00 1414 I
BENZENE < 0 .0050 0.0050 mg/1 PAP 07/20/00 1414
BROM OD I CHLOROM ETHANE 0.0050 0 .0050 mg/1 PAP 07/20/00 1414
BROMOFORM < 0.0050 0.0050 mg/1 PAP 07/20/00 1414
BROMOMETHANE < 0. 010 0.010 mg/1 PAP 07/20/00 1414 I
CARBON DISULFIDE < 0.0050 0.0050 mg/1 PAP 07/20/00 1414
CARBON T8TRACHLORID8 < 0 . 0050 0.0050 mg/1 PAP 07/20/00 1414
CHLOROBENZENE < 0 . 0050 0.0050 mg/1 PAP 07 /20/00 1414 I
CHLOROETHANE < 0.010 0.010 mg/1 PAP 07/20/00 1414
CHLOROFORM < 0.0050 0.0050 mg/1 PAP 07/20/00 1414
CHLOROM8THANE < 0.010 0.010 mg/1 PAP 07/20/00 1414
CIS-1, 2-DICHLOROETHENE < 0.0050 0.0050 mg/1 PAP 07/20/00 1414 I
CI,S-1, 3 -DICHLOROPROPENE < 0.0050 0 .0050 mg/1 PAP 07/20/00 1414
DIBROMOCHLOROMETHANE < 0.0050 0.0050 mg/1 PAP 07/20/00 1414
ETHYLBENZENE < 0.0050 0 .0050 mg/1 PAP 07/20/00 1414
METHYLENE CHLORIDE < 0.0050 0.0050 mg/1 PAP 07/20/00 1414
STYRENE < 0.0050 0. 0050 mg /1 PAP 07/20/00 1414
I
TETRACHLOROETHENE < 0.0050 0 .0050 mg/1 PAP 07/20/00 1414
TOLUENE < 0.0050 0 .0050 mg/1 PAP 07/20/00 1414
TRANS-1,2-DICHLOROETHENE < 0.0050 0 .0050 mg/1 PAP 07/20/00 1414
TRANS-1,3-DICHLOROPROPENE < 0.0050 0 .0050 mg/1 PAP 07/20/00 1414
TRICHLOROETHENE 0.0071 0.0050 mg/1 PAP 07/20/00 1414
VINYL ACETATE < 0.010 0.010 mg/1 PAP 07/20/00 1414
I
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VINYL CHLORIDE < 0.010 0 . 010 mg/1 PAP 07/20/00 1414
XYLENE (TOTAL) < 0.0050 0.0050 mg/1 PAP 07/20/00 1414 I
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E1 ~urst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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DAYIS
FLtlYD LABORATORY ANALYSIS REPORT
Client HNA HOLDINGS INC.
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: PEW-1
Prep Procedure
Analytical Prep Procedures:
BNA SEMIVOLATILF.S
DOWTHERM
Method
.SWS46 3500B
SW846 35008
Analyst Prep Date
MCR 07/20/00
MCR 07/20/00
Project Number: 61195.00-0003
Report Date Augunt 15, 2000
Page 4 of 4
Sample ID L00072001-04
1145
1145
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 \ 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
19
I
DAYIS
FLOYD LABORATORY ANALYSIS REPORT I
Client
Contact
HNA HOLDINGS INC.
!'O BOX 87
SHELBY, NC 28150
,TERRY MCMURRAY
Client ID: PEW-3
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
SW846 9050
Mrit:rix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Semivolatile Organics
SW846 B270C:
1,2,4-TRICHLOROBENZENE
1,2-DICHLOROBENZENE
GW/ChemW
1, 3 -DICl!LOROBENZENE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPIIBNOL
2,4,6-TRICHLOROPHENOL
2,4-DICHLOROPHENOL
2,4-DIMETHYLPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-METHYL-4,6-DINITROPHBNO~
2-METHYLNAPHTHALENE
2-MBTHYLPHENOL
2-NITROANILINE
2-NITROPHENOL
3,3'-DICHLOROBENZIDINE
3-NITROANTLINE
4-BROMOPHENYL PHENYL ETHER
4-CHLOR0-3-MBTHYLPJ-IENOL
4-CHLOROANILINE
4-CHLOROP!18NYL !'HENYL ETHER
4-METHYLPHENOL
4-NITROANILINE
4-NITROPHENOL
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
Result
22.0
6,1
53.0
811.57
< 0.010
< 0,010
< 0.010
< 0.010
< 0.010
< 0.010
< 0.010
< 0.010
< 0. 025
< 0.010
< 0.010
< 0.010
< 0.010
< 0. 025
< 0 .010
< 0. 010
< 0.010
< 0.010
< 0.010
< 0.010
< 0.010
< 0 .,010
< 0.010
< 0.010
< 0.010
< 0. 010
< 0.025
< 0 .010
< o. 010
< 0 .010
Davis & Floyd, lnc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue
20
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Project Number: 61195.00-0003
Report Date Augunt 15, 2000
Page 1 of 4 I
sample ID L00072001-05
Date Collected: 19-JUL-OO 11 : 2 8
Date Received 20-JUL-OO I
Qua.l RDL units Analyst Date Time I
1.0 degrees C 07/19/oo 1120 I
a.so OU 07/19/00 1128
1.0 umho~/cm 07/19/00 1128 I
. 01 feet MSL 07/19/00 1128
I
0.010 mg/1 JRN 07/27/00 1926
0. 010 mg/1 JRN 07/27/00 192 6
0.010 mg/1 JRN 07/27/00 U26 I
0.010 mg/1 JRN 07/27/00 1926
0.010 mg/1 JRN 07/27/00 1926
0.010 mg/1 JRN 07/27/00 1926
o. 010 mgJl JRN 07/27/00 U26 I
0.010 mg/1 JRN 07J27Joo U26
0.025 mg/1 JRN 07/27JOo 1926
0 . 010 mgJl JRN 07J27/00 1926
0 .010 mgJl JRN 07/27Joo 1926 I
0 .010 mgJl JRN 07J27JOO 1926
0 .010 mg/1 JRN 07/27JOo 1926
0 .025 mgJl JRN 07J27JOO 1926 I
0. 010 mg/1 JRN 07/27JOO 1926
0.010 mgJl JRN 07J27/00 1926
0 .010 mg/1 JRN 07 /21 Joo 1926
0. 010 mg/1 JR.N 07/27/00 1926 I
0.010 mg/1 JRN o7 /27 Joo 1926
0.010 mg/1 JRN 07/27/00 1926
0.010 mgJl JRN 01/27/oo U26
0. 010 mg/1 JRN 07J27JOo 1926 I
0 . 010 mg/1 JRN 07/27/00 1926
0.010 mg/1 JRN 07/27JOO 1926
0 .010 mg/1 JRN 07/27JOO 1926 I
0.010 mg/1 JRN 07/27/00 1926
0 .025 mgJl JRN 07J27J00 1926
0.010 mg/1 JRN 07/27/00 1926
0.010 mgJl JRN 07J27/0o 1926 I
0 .010 mg/1 JRN 07/27/00 1926
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I Greenwood, SC 29649 I (864i 229-4413 I Fax [phone]
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
c,:,ntact
HNA HOLDINGS INC.
PO BOX 87
.SHELBY, NC 28150
JERRY MCMURRAY
Client ID: PEW-3
Parameter
BENZO (A) A.NTHRACENE
BENZO (A) PYP.ENE
BENZO(B)fLUORANTl!ENE
BENZO (G, H, I) PERYLENB
BENZO ( I<.) FLUORANTHENE
BENZOIC ACID
BENZYL ALCOHOL
BIS(2-CHLOROETHOXY)MBTHANE
BIS(2-CHLOROETHYL)ETHBR
BIS(2-CHLOROJ.'JOPROPYL)BTHER
BIS(2-ETHYLHBXYL)PHTHALATE
BUTYL BENZYL PHTHALATE
CHRYSENE
DI-N-B\JTYL PHTHALATE
Dl-N-OCTYL PHTHALATE
DIBENZ (A, H) ANTl-lRACENE
DIBENZOFURAN
DIETHYL PHTHALATE
DIMETHYL PHTHALATE
FLUORANTHENB
FLUORENE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROCYCLOPENTADIBNE
HEXACHLOROETHANE
INOENO(l,2,3-CD)PYRENB
ISOPHORONE
N-NITROSODI-N-PROPYLAMINE
N-NITR0.<30D I PHENYLAM INE
NAPHTHALENS
NITROBBNZENE
PBNTACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRENE
SWB46 8270C DOWTHERf,J
1,1'-BIPHENYL
BIPHENYL ETHEP.
Reault
< 0 .010
' o. 010
< 0.010
< 0 .010
< 0.010
< 0 .050
' 0 .010
< 0.010
0 .010
< 0. 010
< 0 .010
< o. 010
' 0 .010
< 0.010
' o. 010
< 0.010
< 0.010
< 0 .010
' 0 .010
< 0. 010
< 0.010
' 0 .010
< 0. 010
< 0.010
< 0.010
< 0 .010
< 0 .010
< o. 010
< o. 010
< 0.010
< 0.010
< 0.025
< o. 010
< 0 .010
< 0.010
< 0. 010
< 0.010
Project Number: 61195 .00-0003
Report Date August 15, 2000
Page 2 of 4
Sample ID L00072001-0S
Qual RDL Units Analyst Data Time
0.010 mg/1 JRN 07/27/00 1926
0 .010 mg/1 JRN 07/27/00 1926
0 .010 mg/1 JRN 07/27/00 1926
0.010 mg/1 JRN 07/27/00 1926
0 .010 mg/1 JRN 07 /27 /00 1926
0 .050 mg/1 JRN 07/27/00 1926
0.010 mg/1 JRN 07 /27 /oo 1926
0 .010 mg/1 JRN 07/27/00 1926
0 .010 mg/1 JRN 07/27/00 1926
0. 010 mg/1 JRN 07/27/00 1926
0.010 mg/1 JRN 07/27/00 1926
0. 010 mg/1 JRN 07/27/00 1926
0.010 mg/1 JRN 01i27/00 1926
0.010 mg/1 JRN 07/27/00 1926
0 .010 mg/1 JRN 01/27/oo 1926
0.010 mg/1 JRN 07/27/00 1926
0. 010 mg/1 JRN 07/27/00 1926
0.010 mg/1 JRN 07/27/00 1926
0 .010 mg/1 JRN 07/27/00 1926
0 .010 mg/1 JRN 07/27/00 1926
0.010 mg/1 JRN 07/27/oo 1926
0.010 mg/1 JRN 07/27/00 1926
0 .010 mg/1 JRN 07/27/00 1926
0. 010 mg/1 JRN 07/27/00 1926
0. 010 mg/1 JRN 07/27/00 1926
0.010 mg/1 JRN 07/27/00 1926
0.010 mg/1 JRN 07/27/00 1926
0 .010 mg/1 JRN 07/27/00 1926
0.010 mg/1 JRN 07/27/00 1926
0.010 mg/1 JRN 07/27/00 1926
0. 010 mg/1 JRN 07/27/00 1926
0.025 mg/1 JRN 07/27/00 1926
0.010 mg/1 JRN 07/27/00 1926
0 .010 mg/1 JRN 07/27/00 1926
0.010 mg/1 JRN 07/27/00 1926
0.010 mg/1 JRN 01/21/00 1926
0 .010 mg/1 JRN 07/27/00 1926
Davis & Floyd, Inc. I PO Drawer 428 l Greenwood, SC 29646 I 616 E. Durst Avenue I Greenwood, SC 29649 I [phone] ! Fax [phone]
21
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D~S FL D LABORATORY ANALYSIS REPORT I
I
Client HNA HOLDINGS INC. Project Number: 61195.00-0003
PO EOX 87
GHELBY, NC 28150 Report Date Augunt 15, 2000
Cc;,ntnct JERRY MCMURRAY Page 3 of , I
r:lient IO; PEW-3 Sample ID L00072001-05 I
Pararnater Raoult Qual RDL Unite Analyst Date Time
Volatile Organics
SW846 8260B I
1,1,1-TRICHLOROETHANE ' 0.0050 0 .0050 mg/1 PAP 07/20/00 1439
1,1,2,2-TETRACHLOROETHANE ' 0.0050 0 .0050 mg/1 PAP 07/20/00 1439
1,1,2-TRICHLOROETHANE ' 0.0050 0 .0050 mg/1 PAP 07/20/D0 1439
1, 1-DICHLOROETJ-IANE ' 0.0050 0 .0050 mg/1 PAP 07/20/00 1439 I
1,1-DlCHLOROETHENE ' 0.0050 0 .0050 mg/1 PAP 01/20/00 1439
1,2-DICHLOROETHANE ' 0.0050 0 . 0050 mg/1 PAP 07/20/00 1439
1, 2-0ICHLOROPROPANE ' 0.0050 0.0050 mg/1 PAP 07/20/00 1439 I
2-BUTANONE ' 0.010 0 .010 mg/1 PAP 07/20/00 1439
2-HEXANONE ' 0.010 0 .010 mg/1 PAP 07/20/00 143 9
4-METHYL-2-PENTANONE ' 0.0050 0.0050 mg/1 PAP 07/20/00 1439
ACETONE ' 0.010 0.010 mg/1 PAP 01i20/oo 1439 I
BENZENE ' 0.0050 0.0050 mg/1 PAP 01/20/00 1439
BROMODICHLOROMETHANE ' 0.0050 0.0050 mg/1 PAP 07/20/00 1439
BROMOFORM ' 0.0050 0 .0050 mg/1 PAP 01/20/00 1439
BROMOMETHANE ' 0.010 0.010 mg/1 PAP 07/20/00 1439 I
CARBON DI:JULFIDE ' 0. 0050 0 .0050 mg/1 PAP 07/20/00 1439
CARBON TETRACHLORIDE ' 0.0050 0.0050 mg/1 PAP 07/20/00 1439
CHLOROBENZENE ' 0.0050 0 .0050 mg/1 PAP 01/20/00 1439
CHLOROETHANE ' 0.010 0.010 mg/1 PAP 01/20/00 1439 I
CHLOROFORM ' 0.0050 0.0050 mg/1 PAP 01/20/00 1439
CHLOROMETHANE ' 0.010 0. 010 mg/1 PAP 01/20/00 1439
CIS-1, 2-DICHLOROETHENE ' 0.0050 0 .0050 mg/1 PAP 01/20/00 1439 I
CIS-1, 3 -DICHLOROPROPENE ' 0.0050 D . 0050 mg/1 PAP 07/20/00 1439
DIBROMOCHLOROMETHANE ' 0.0050 0 .0050 mg/1 PAP 07/20/00 1439
ETHYLBENZENE ' 0.0050 0.0050 mg/1 PAP 07/20/00 1439
METHYLENE CHLORIDE ' 0.0050 0. 0050 mg/1 PAP 07/20/00 1439 I
STYRENE ' 0 .0050 0.0050 mg/1 PAP 01/20/00 143 9
TBTRACHLOROSTl!ENE ' 0 . 0050 0 .0050 mg/1 PAP 07/20/00 1439
TOLUENS ' 0.0050 0.0050 mg/1 PAP 07/20/00 1439
TRANS-1,2-DICHLOROETHENE ' 0.0050 0 .0050 mg/1 PAP 07/20/00 1.439 I
TRANS-1,3-DICHLOROPROPSNE ' 0.0050 0.0050 mg/1 PAP 01/20/00 1439
TRICHLOROETHENE ' 0.0050 0 . 00 50 mg/1 PAP 07/20/00 1439
VINYL ACETATE ' 0 .010 0 .010 mg/1 PAP 01/20/00 1439 I
VINYL CllLORIPE ' 0.010 0.010 mg/1 PAP 01/20/00 1'139
XYLENE (TOTAL) ' 0.0050 0.0050 mg/1 PAP 01/20/00 1439 I
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E2 2urst Avenue I Greenwood, SC 29649 I [phone] l Fax [phone]
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
PO BOX 87
,'::HELBY, NC 28150
,TERRY MCMURRJ\Y
Client ID: PE:W-3
Prep Procedure
Analytical Prep Procedures:
BNA .SEMIVOL.ATILEC.:
DOWTHERM
Method
.SWB46 35008
.SWB46 3500B
Project Number: 61195.00-0003
Report Date Al1gu.st 15, 2000
Page 4 of 4
Sample ID L00072001-05
Analyst Prep Date
MCR 01/20/00 1145
MCR 07/20/00 1145
Davis & Floyd, Inc. l PO Drawer 428 I Greenwood, SC 29648 \ 816 E. Durst Avenue I Greenwood, SC 29649 I (864i 229-4413 I Fax [phone]
23
D1\YIS
FLOYD LABORATORY ANALYSIS REPORT
Client
contact
HNA HOLDINGS INC,
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: PEW-3 DUP,
Parameter
Field Data
EPA 170. l
TEMPERATURE
SW84.6 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Semivolatile Organics
GW/ChemW
SW846 8270C
1,2,4-TRICHLOROBENZENE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DICHLOROPHENOL
2,4-DIMETHYLPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHBNOL
2-METHYL-4,6-DINITROPHENOL
2-METHYLNAPHTHALENE
2-METHYLPHENOL
2-NITROANILINE
2-NITROPHBNOL
3,3'-DICHLOROBENZIDINE
3-NITROANILINE
4-BROMOPHENYL PHENYL ETHER
4-CHLOR0-3-METHYLPHENOL
4-CHLOROANILINE
4-CHLOROPHENYL PHBNYL ETHER
4-METHYLPHENOL
4-NITROANILINE
4-NITROPIIENOL
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
Result
22.0
6,1
53,0
811.57
< 0. 010
< o. 010
< 0 .010
< 0.010
< 0.010
< 0. 010
< 0.010
< 0.010
< 0.025
' 0.010
< 0. 010
' 0.010
' 0. 010
< 0.025
' 0.010
' o. 010
' 0 .010
' 0. 010
' 0.010
' 0.010
' 0.010
' 0.010
< 0.010
< 0.010
' 0 .010
' 0. 010
< 0. 025
< 0 .010
< 0.010
< 0. 010
Project Number: 61195.00-0003
Report Date Augu:::t 15, 2000
Page 1 of 4
Sample ID L00072D01-06
Date Collected: 19-JUL-OO 11: 28
Date Received 20-JUL-00
Qual RDL Unite Analyst Date Time
l.O degreen C 07/19/00 1128
0.50 OU 07/19/00 1128
1.0 umhos/cm 07/19/00 1128
. 01 feet MSL 07/19/00 1128
0.010 mg/1 JRN 07/27/00 2003
o. 010 mg/1 JRN 07 /27 /oo 2003
0 .010 mg/1 JRN 07/27/00 2003
0.010 mg/1 JRN 07/27/00 2003
0.010 mg/1 JRN 07/27/00 2003
0 .010 mg/1 JRN 07/27/00 2003
0 .010 mg/1 JRN 07/27/00 2003
0 .010 mg/1 JRN 07/27/00 2003
0. 025 mg/1 JRN 07/27/00 2003
0.010 mg/1 JRN 07/27/00 2003
0.010 mg/1 JRN 07/27/00 2003
0.010 mg/1 JRN 07/27/00 2003
0.010 mg/1 JRN 07/27/00 2003
0. 025 mg/1 JRN 07/27/00 2003
0.010 mg/1 JRN 07/27/00 2003
0.010 mg/1 JRN 07/27/00 2003
0 .010 mg/1 JRN 07/27/00 2003
0 .010 mg/1 JRN 07/27/00 2003
0 .010 mg/1 JRN 07/27/00 2003
0.010 mg/1 JRN 07/27/00 2003
0.010 mg/1 JRN 07/27/00 2003
0.010 mg/1 JRN 07/27/00 2003
0.010 mg/1 JRN 07/27/00 2003
0. 010 mg/1 JRN 07/27/00 2003
0 .010 mg/1 JRN 07/27/00 2003
0.010 mg/1 JRN 07/27/00 2003
0.025 mg/1 JRN 07/27/00 2003
0.010 mg/1 JRN 07/27/00 2003
0 .010 mg/1 JRN 07/27/00 2003
0.010 mg/1 JRN 07/27/00 2003
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E2 4urst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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D~S LABORATORY ANALYSIS FL D REPORT
I Client HNA HOLDINGS INC, Project Number: 61195.00-0003
PO BOX 87
.SHELBY, NC 28150 Report Date Augunt 15, 2000
Cc,ntact ,TERRY MCMURRAY Page 2 of 4
I Client ID: PEW-3 DUP. Sample ID L00072001-06
I
Parameter Result Qual RDL Unite Analyst Date Time
BENZO(A)ANTHRACENE < 0.010 0 .010 mg/1 JRN 07/27/00 2003
BENZO (A} PYRENE < 0 .010 0 . 010 mg/1 ,TRN 07/27/oo 2003
I BENZO (B) FLUORANTHENE < 0 .010 0.010 mg/1 JRN 07/27/00 2003
BENZO(G,H,I)PERYLENE < 0.010 0 .010 mg/1 JRN 07/27/00 2003
BENZO(K)FLUORANTHENE < 0. 010 0 .010 mg/1 JRN 07/27/00 2003
BENZOIC ACID < 0.050 0 .oso mg/1 JRN 07/27/00 2003
I BENZYL ALCOHOL < 0.010 0.010 mg/1 JRN 01 /21 /oo 2003
BIS (2-CHLOROETHO:--::Y) METHANE < 0. 010 0.010 mg/1 JRN 07/27/00 2003
BIS(2-CHLOROETHYL)ETHER < 0 .010 0. 010 mg/1 JRN 07/27/00 2003
BIS(2-CHLOROJ.'JOPROPYL)ETHER < 0.010 0 .010 mg/1 JRN 07/27/00 2003
I BIS { 2-ETHYLHEXYL) PHTHALATE < 0.010 0.010 mg/1 JRN o7 /27 Joo 2003
BUTYL BENZYL P!!THALATE < 0 .010 0 .010 mg/1 JRN 07/27/00 2003
CHRYSENE < 0. 010 0.010 mg/1 JRN 07/27/00 2003
I DI-N-BUTYL PHTHALATE < 0 .010 0.010 mg/1 JRN 07/27/00 2003
DI-N-OCTYL PHTHALATE < 0.010 0.010 mg/1 JRN 07/27/00 2003
DIBENZ(A,H)ANTHRACENE < 0 .010 0 . 010 mg/1 JRN 07/27/00 2003
DIBENZOFURAN < 0. 010 0.010 mg/1 JRN 07/27/00 2003
I DIETHYL PHTHALATE < 0.010 0.010 mg/1 JRN 07/27/00 2003
DIMETHYL PHTHALATE < 0 .010 0.010 mg/1 JRN 07/27/00 2003
FLUORANTHENE < 0 .010 0 .010 mg/1 JRN 07/27/00 2003
FLUORENE < 0. 010 0 .010 mg/1 JRN 07/27/00 2003
I HEXACHLOROBENZENE < 0.010 0 .010 mg/1 JRN 07/27/00 2003
HEXACHLOROBUTADIENE < 0.010 0.010 mg/1 JRN 01 /27 /oo 2003
HEXACHLOROCYCLOPENTADIENE < 0.010 0 .010 mg/1 JRN 07/27/00 2003
I HEXACHLOROETHANE < 0.010 0.010 mg/1 JRN 07/27/00 2003
INDENO(l, 2, )-CD) PYRENE < 0.010 0.010 mg/1 JRN 07/27/00 2003
ISOPHORONE < 0.010 0 .010 mg/1 JRN 07/27/oo 2003
N-NITROSODI-N-PROPYLAMINE < 0 .010 0. 010 mg/1 JRN 07/27/00 2003
I N-NITROSODIPHENYLAMINE < o. 010 0 .010 mg/1 JRN 01 /27 /oo 2003
NAPHTHALENE 0 .010 0 .010 mg/1 JRN 07/27/00 2003
NITROBENZENE < 0. 010 0 .010 mg/1 JRN 07/27/00 2003
PENTACHLOROPHENOL < 0.025 0 .025 mg/1 JRN 01/21/00 2003
I PHENANTHRENE < 0.010 0.010 mg/1 JRN 07/27/00 2003
PHENOL < 0.010 0 .010 mg/1 JRN 07/21/00 2003
PYRENE < 0.010 0.010 mg/1 JRN 07/27/00 2003
I SW846 8270C DOWTHEPJ-1
1, 1' -BIPHENYL < 0.010 0.010 mg/1 JRN 07/27/00 2003
BIPHENYL ETHER < 0. 010 0. 010 mg/1 JRN 07/27/00 2003
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I Davis & Floyd, Inc. \ PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue 25 I Greenwood, SC 29649 I [phone] I Fax [phone]
I
D~S FL D LABORATORY ANALYSIS REPORT I
I
client HNA HOLDINGS INC. Project Number: 61195.00-0003
PO EOX 87
::',HELBY, NC 28150 Report Date Augu:::;t 15, 2000
Cont:.ict .TERR.i MCMURRAY Page 3 of 4 I
Cli-2nt ID: PEW-3 OUP. Sample ID L00072001-06
Parameter Result Qual RDL Uni ta Analyst Date Time I
Volatile Organics
SW846 8260B I
1,1,1-TRICHLOROETHANE ' 0.0050 0 .0050 mg/1 PAP 07/20/00 1503
1,1,2,2-TETRACHLOROETHANE < 0 . 0050 0 .0050 mg/1 PAP 07/20/00 1503
1, 1,2-TRICHLOROETHANE < 0, 0050 D. 0050 mg/1 PAP 07/20/00 1503
1,1-DICHLOROETHANE < 0.0050 0 .ooso mg/1 PAP 07/20/00 1503 11
1,1-DICHLOROETHENE < 0.0050 D .0050 mg/1 PAP 07/20/00 1503
1,2-DICHLOROETHANE ' 0.0050 0 .0050 mg/1 PAP 07/20/00 1503
1,2-DICHLOROPROPANE < 0.0050 0.0050 mg/1 PAP 07/20/00 1503
2-BUTANONE < 0 .010 0.010 mg/1 PAP 07/20/00 1503 I
2-HEXANONE < 0. 010 0.010 mg/1 PAP 07/20/00 1503
4-METHYL-2-PENTANONE < 0.0050 0.0050 mg/1 PAP 07/20/00 1503
ACETONE < 0.010 0.010 mg/1 PAP 07/20/00 1503 I
BENZENE < 0.0050 0.0050 mg/1 PAP 07/20/00 1503
BROMODICHLOROMETHANE < 0.0050 0 . 0050 mg/1 PAP 07/20/00 1503
BROMOFORM 0.00S0 0.0050 mg/1 PAP 07/20/00 1503
BROMOMETHANE ' 0.010 0.010 mg/1 PAP 07/20/00 1503 I
CARBON DI.SULFIDE ' 0.0050 0.0050 mg/1 PAP 07/20/00 1503
CARBON TETRACHLORIDE < 0.0050 0.0050 mg/1 PAP 07/20/00 1503
CHLOROBENZENE < 0.0050 .0050 mg/1 PAP 07/20/00 1503
CHLOROETHANE < 0.010 0.010 mg/1 PAP 07/20/00 1503 I
CHLOROFORM < 0.0050 0.0050 mg/1 PAP 07/20/00 1503
CHLOROMETHANE < 0.010 0. 010 mg/1 PAP 07/20/00 1503
CIS-1,2-DICHLOROETHENE < 0.0050 0.0050 mg/1 PAP 07/20/00 1503
CIS-1,3-DICHLOROPROPENE < 0 .0050 0 . 0050 mg/1 PAP 07/20/00 1503 I
DIBROMOCHLOROMETHANE < 0.0050 o. 0050 mg/1 PAP 07/20/00 1503
ETHYLBENZENE < 0.0050 0 .0050 mg/1 PAP 07/20/00 1503
METHYLENE CHLORIDE < 0.0050 0.0050 mg/1 PAP 07/20/00 1503 I
STYRENE < 0.0050 0 .ooso mg/1 PAP 07/20/00 1503
TETRACHLOROETHENE < 0.0050 0. 0050 mg/1 PAP 07/20/00 1503
TOLUENE 0.0050 0 .0050 mg/1 PAP 07/20/00 1503
TRANS-1,2-DICHLOROETHENE < 0.0050 0 .0050 mg/1 PAP 07/20/00 1503 I
TRANS-1,3-DICHLOROPROPENE < 0.0050 0 . 0050 mg/1 PAP 07/20/00 1503
TRICHLOROETHENE < 0.0050 0 .0050 mg/1 PAP 07/20/00 1503
VINYL ACETATE < 0.010 0.010 mg/1 PAP 01/20/00 1503
VINYL CHLORIUE < 0.010 0.010 mg/1 PAP 07/20/00 1503 I
XYLENE (TOTAL) < 0.0050 0.0050 mg/1 PAP 07/20/00 1503
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 ] 816 E. Durst Avenue
26
I Greenwood, SC 29649 I [phone] I Fax [phone]
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Di\YIS
FLo'YD
client
C:c,ntact
Client
Prep Procedure
ID:
Analytical Prep Procedures:
BNA .SEMIVOLATII,E.S
DOWTHERM
LABORATORY ANALYSIS REPORT
HNA HOLDINGS INC.
PO BOX 87
SHELBY, NC 28150
,1ERRY
PEW-3
MCMURRAY
CUP,
Method
SW846 3500B
:JWB46 3500B
Project Number: 61195.00-0003
Report Date Augu::it 15, 2000
Page 4 of 4
Sample ID L00072001-06
Analyst Prep Date
MCR 07/20/00 1145
MCR 07/20/00 1145
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 \ (864). 229-4413 I Fax [phone]
27
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DAYIS
FLtJ\'D LABORATORY ANALYSIS REPORT I
Client
Contact
HNA HOLDINGS INC,
PO BOX 87
.>HELBY, NC 28150
JERRY I-ICMURRAY
~lient ID: PEW-4
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
SWB46 9050
11,1trix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Semivolatile Organica
SWB46 B270C
1,2,4-TRICHLOROBENZENE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-0ICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DICHLOROPHENOL
2,4-DIMETHYLPHENOL
2, 4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-METHYL-4,6-DINIT~OPHENOL
2-METHYLNAPHTHALENE
2-METHYLPHENOL
2-NITROANILINE
2-NITROPHENOL
3,3'-DICHLOROBENZIDINE
3-NITROANILINE
4-BROMOPHENYL PHENYL ETHBP.
4-CHLORO-3 -METlriLPHENOL
4-CHLOROANI LHJE
4-CHLOROPHENYL PHENYL ETHER
4-METHYLPHENOL
4-NITROANILINE
4-NITROPHENOL
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
Result
21.0
5.5
84. 0
813.39
0.010
< 0.010
< 0.010
< 0 .010
< 0. 010
< 0.010
< 0.010
< o. 010
< 0 .025
< 0.010
< 0. 010
< 0.010
< 0. 010
< 0.025
< 0.010
< 0.010
< 0.010
< 0.010
< 0.010
< 0. 010
< 0.010
< 0 .010
< 0 .010
< 0.010
< 0.010
< 0.010
< 0. 025
< 0.010
< 0. 010
< 0.010
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 l 816 E. Durst Avenue
28
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Project Number: 61195.00-0003
Report Date Auguot 15, 2000
Page 1 of 4 I
Sample ID L000720D1-07
Date Collected: El-JUL-CO 12 : 00
Date Received 20-JUL-OO
I
Qual RDL Units Analyst Date Tirne I
1.0 degreen c 07/19/00 1200 I
0.50 OU 07/19/00 1200
1 . 0 umhoo/cm 07/19/00 1200 I
.01 feet MSL 07/19/00 1200
I
0 .010 mg/1 JRN 07/27/00 2040
o. 010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 01/21/00 2040 I
0 .010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0. 010 mg/1 JRN 07/27/00 2040
0 .010 mg/1 JRN 07/27/00 2040 I
0. 010 mg/1 JRN 01 /21 /oo 2040
0 . 025 mg/1 JRN 07/27/00 2040
0 ,010 mg/1 JRN 01/21/00 2040 I
0.010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0. 025 mg/1 JRN 07/27/00 2040 I
0 .010 mg/1 JRN 01/21/00 2040
0. 010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0 .010 mg/1 JRN oi/21/00 2040 I
0.010 mg/1 JRN 07/27/00 2040
o. 010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 01/21/00 2040
0 .010 mg/1 JRN 07/27/00 2040 I
0 .010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 01/21/00 2040
0 .010 mg/1 JRN 07/27/00 2040 I
0. 010 mg/1 JRN 07/27/00 2040
0 .025 mg/1 JRN 07/27/00 2040
0 .010 mg/1 JRN 07/27/00 2040
0 .010 mg/1 JRN 01/21/00 2040 I
0.010 mg/1 JRN 07/27/00 2040
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I Greenwood, SC 29649 I [phone] I Fax [phone]
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
,:·,:,ntact
HNA HOLDINas INC.
PO sm: 87
:.iHELBY, NC 28150
,TERRY MCMURRAY
<_'lient ID: PEW-4
Parameter
BENZO{A)ANTHRACENE
BENZO(A)PYRENE
BENZO(B)FLUORANTHENE
BENZO(G,H,I}PERYLENE
BENZO(K)FLUORANTHENE
BENZOIC ACID
BENZYL ALCOHOL
BIS ( 2 -CHLOROETl!OX"i) METHANE
BIS(2-CHLOROETHYL)ETHER
BI.S (2-CHLOROI.S'OPROPYL) ETHER
BIS{2-ETHYLHEXYL)PHTHALATE
BUTYL BENZYL PHTHALATE
CHRYSENE
DI-N-BUTYL PHTHALATE
DI-N-OCTYL PHTHALATE
DIBENZ(A,H)ANTHRACENE
DIBENZOFURAN
DIETHYL PHTHALATE
DIMETHYL PHTHAL.-).TE
FLUORANTHENE
FLUORENE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROCYCLOPENT.lilllENE
HEXACHLOROETHANE
INDENO(l,2,3-CD)PYRENE
ISOPHORONE
N-NITROSODI-N-PROPYLAMINE
N-NITRO.SOD I PHENYLAM INE
NAPHTHALENE
NITROBENZENE
PENTACHLOROPHENOL
PHENJ..NTHRENE
PHENOL
PYRENE
SW846 8270C DOViTHEP.M
1,1'-BIPHENYL
BIPHENYL ETHER
Result
< 0.010
< 0.010
0. 010
< 0. 010
< o. 010
< 0.050
< 0.010
< 0.010
< 0 .010
< 0. 010
< 0 .010
< 0 . 010
< 0, 010
0.010
< 0.010
< 0 .010
0.010
< 0.010
< 0.010
< 0' 010
< 0.010
< 0.010
< o. 010
< 0. 010
< 0. 010
< 0.010
< 0.010
< 0.010
< 0 .010
< o. 010
< 0.010
< 0.025
< 0.010
< 0.010
< o. 010
0.012
0.041
Project Number: 61195.00-0003
Report Date Augu~t 15, 2000
Page 2 of '
Sample ID L00072001-07
Qua.l RDL Unite Ana.lyat Date Time
0.010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0.010 rng/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0.050 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0 .010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2 04 0
0 .010 mg/1 JRN 07/27/00 2040
0. 010 mg/1 JRN 07/27/00 2040
0 .010 mg/1 JRN 07/27/00 2040
0, 010 mg/1 JRN 07 i21 /oo 2040
0. 010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0 .010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0. 010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0 .010 mg/1 JRN 07/27/00 2040
0 .010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0 .010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0 .010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0. 010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0.025 mg/1 JRN 07/27/00 2040
0 .010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0.010 mg/1 JRN 07/27/00 2040
0 .010 mg/1 JRN 07/27/00 2040
0. 010 mg/1 JRN 07/27/00 2040
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 ! 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
29
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Di\YIS
FLtJ\'D LABORATORY ANALYSIS REPORT I
Client
Contc1ct
HNA HOLDINGS INC.
PO Bo>: 87
SEELEY, NC 28150
,TERRY MCMURRAY
Client ID: PEW-4
Parameter
Volatile Organics
SW846 8260B
1, 1, !-TRICHLOROETHANE
1, 1, 2 ,:2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1, 1-DICHLOROETH!'\NE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPA.NE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOP.OMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISUU'IDE
CARBON TBTP.ACHLORIDE
CHLOROBENZENE
CHLOROETHltNE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DlCHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1, 2-DICHLOROETHENE
TRANS-1, :, -DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I
Result
0 .0050
< 0 .0050
< 0 .0050
< 0 .0050
< 0. 0050
< 0 .0050
< 0 . 0050
< 0. 010
< 0 .010
< 0.0050
< 0.010
< 0 .0050
< 0 .0050
0 . 0050
< 0.010
< 0.0050
< 0. 0050
0. 0050
< 0.010
< 0.0050
< 0.010
0.0080
< 0.0050
< 0.0050
< 0 .0050
< 0. 0050
< 0 .0050
< 0. 0050
< o. 0050
< 0.0050
< 0.0050
0.053
< 0 .010
< 0 .010
< 0.0050
816 E. Durst Avenue
30
Project Number: 61195.00-0003
Report Date
Page 3 of 4
Auguat 15, 2000
Sample ID L00072001-07
Qual RDL Units Analyst Date
0 .0050 mg/1 PAP 07/20/00
0 . 0050 mg/1 PAP 07/20/00
0 .0050 mg/1 PAP 07/20/00
0 . 00 50 mg/1 PAP 07/20/00
0. 0050 mg/1 PAP 07/20/00
0 .0050 mg/1 PAP 07/20/00
0 .0050 mg/1 PAP 07/20/00
o. 010 mg/1 PAP 01/20/00
0 .010 mg/1 PAP 07/20/00
0.00S0 mg/1 PAP 07/20/00
0.010 mg/1 PAP 07/20/00
0. 0050 mg/1 PAP 07/20/00
0 .00S0 mg/1 PAP 07/20/00
0. 0050 mg/1 PAP 07/20/00
0.010 mg/1 PAP 07/20/00
0 .0050 mg/1 PAP 07/20/00
0 .0050 mg/1 PAP 07/20/00
0. 0050 mg/1 PAP 07/20/00
0.010 mg/1 PAP 07/20/00
0.0050 mg/1 PAP 07/20/00
0. 010 mg/1 PAP 07/20/00
0 .0050 mg/1 PAP 07/20/00
0 . 00 5 0 mg/1 PAP 07/20/00
0 .0050 mg/1 PAP 07/20/00
0 .0050 mg/1 PAP 07/20/00
0. 00S0 mg/1 PAP 07/20/00
0 .0050 mg/1 PAP 07/20/00
0. 0050 mg/1 PAP 07/20/00
0 .0050 mg/1 PAP 07/20/00
0.0050 mg/1 PAP 07/20/00
0 .0050 mg/1 PAP 07/20/00
0 . 00 50 mg/1 PAP 07/20/00
0 .010 mg/1 PAP 07/20/00
0 .010 mg/1 PAP 07/20/00
0.0050 mg/1 PAP 07 /20/00
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Time
I
1527
152 7
1527
1527 I
1527
1527
1527
1527 I
1527
1527
1S27 I
1527
1S27
1527
1527 I
1527
1527
1527
1527 I
1527
1527
1S27 I 1527
1527
1527
1527 I
1527
1527
1527
1527 I
1527
1527
1527
1527 I
1527
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DAYIS
FLO\'D LABORATORY ANALYSIS REPORT
Client
,_::,)ntact
HNA HOLDINGS INC.
PO BOX 87
.SHELBY, NC 28150
,TERRY f·iCMURRAY
<lient ID: PEW-4
Prep Procedure
Analytical Prep Pi:ocedures:
BNA ,SEMIVOLATI LE1:;
DOWTHERM
Method
SWS46 3500B
:3WB46 35008
Project Number: 61195.00-0003
Analyst Prep Date
Report Date
Page 4 of 4
Sample ID
MCR 07/20/00 1145
MCR 07/20/00 1145
Auguot 15, 2000
L00072001-D7
Davis & Floyd, 1nc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
31
I
DAYIS
FLOYD LABORATORY ANALYSIS REPORT I
Client
Contact
HNA HOLDINGS INC.
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: F-55
Parameter
Field Data
EPA 170.l
TEMPERATURE
SW846 9040B
PH
SW846 9050
Mntrix
SPECIPIC CONDUCTIVITY
GROUND WATER ELEVATION
Semivolatile Organica
SW846 B270C
1,2,4-TRICHLOROBENZENE
1,2-0ICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4,S-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DICHLOROPHENOL
GW/ChemW
2, 4-DIMETHYL PHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-METHYL-4,6-DINITROPHENOL
2-METHYLNAPHTHALENE
2-METHYLPHENOL
2-NITROANILINE
2-NITROPHENOL
3,3'-DICHLOROBENZIDINE
3-NITROANILINE
4-BROMOPHENYL PHENYL ETHER
4-CHLOR0-3 -METllYLPHENOL
4-CHLOROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-METHYLPHENOL
4-NITROANILINE
4-NITROPHENOL
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
Reault
21.0
6.l
275
810.56
< 0.050
< 0.050
< 0.050
< 0.050
< 0.050
< 0.050
< 0.050
< 0.050
< 0,13
< 0.050
< 0 .050
< 0 .050
< 0.050
< 0 .13
< 0.050
< 0.050
< 0.050
< 0. 050
< 0.050
< 0.050
< 0.050
< 0.050
< 0 .050
< o. 050
0 .11
< 0.050
< 0,13
< 0. 050
< 0.050
< 0,050
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue
32
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P·roject Number: 61195. 00-0003
Report Date Augu::;t 15, 2000
Page 1 of 4 I
Sample ID L0007200l-08
Date Collected: 19-JUL-OO 11 :SO I
Date Received 20-JUL-OO
Qual RDL Onita Analyst Date Time I
1.0 degreeo C 07/19/00 1150 I
0.50 OU 07/19/00 1150
1.0 umho::;/cm 07/19/00 1150 I
.01 feet MSL 07/19/00 1150
I
X 0 .050 mg/1 JRN 01/21/00 2117
X 0.050 mg/1 JRN 07/27/00 2117
X 0 .050 mg/1 JRN 07/27/00 2117 I
X 0.050 mg/1 JRN 07/27/00 2117
X 0.050 mg/1 JRN 07/27/00 2117
X 0.050 mg/1 JRN 07/27/00 2117
X 0.050 mg/1 JRN 01/21/00 2117 I
X 0.050 mg/1 JRN 07/27/00 2117
X 0.13 mg/1 JRN 07/27/00 2117
X 0.050 mg/1 JRN 07/27/00 2117 I
X 0.050 mg/1 JRN 07/27/00 2117
X 0.050 mg/1 JRN 07/27/00 2117
X 0 .050 mg/1 JRN 07/27/00 2117
X 0 .13 mg/1 JRN 07/27/00 2117 I
X 0.050 mg/1 JRN 07/27/00 2117
X 0.050 mg/1 JRN 07/27/00 2117
X 0 .050 mg/1 JRN 07/27/00 2117
X 0 .050 mg/1 JRN 01/21/00 2117 I
X 0. 050 mg/1 JRN 07/27/00 21.17
X 0. 050 mg/1 JRN 07/27/00 2117
X 0.050 mg/1 JRN 07/27/00 2117
X 0.050 mg/1 JRN 07/27/00 2117 I
X 0.050 mg/1 JRN 07/27/00 2117
X 0.050 mg/1 JRN 07/27/00 211. 7
0 .050 mg/1 JRN 07/27/00 2117 I
X 0.050 mg/1 JRN 07/27/00 2117
X 0.13 mg/1 JRN 07/27/00 2117
0. 050 mg/1 JRN 07/27/00 2117
X 0. 050 mg/1 JRN 01/21/00 2117 I
X 0.050 mg/1 JRN 07/27/00 2117
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client HUA HOLDINGS INC, Project Number: 61195. 00-0003
PO BOX 87
,SHELBY, NC 2 8150 Report Date Auguct lS, 2000
rontc1ct ,TERRY rKMURRAY Page 2 of '
Client ID: F-55 Sample ID L00072001-08
Parameter Result Qual RDL Units Analyst Date Time
BENZO(A)ANTHRACENE < 0. 050 X 0.050 mg/1 JRN 07/27/00 2117
BENZO (A) P'iRENE < 0, 050 X o.oso mg/1 JRN 07/27/00 2117
BENZO(B)FLUORANTHENE < 0 .050 X 0 .oso mg/1 JRN 07/27/00 2117
BENZO(G,H,I)PERYLENE < 0.050 X 0.050 mg/1 JRN 07/27/00 2117
BENZO (K) FLUORANTHENE < 0.050 X o.oso rng/1 JRN 07/27/00 2117
BENZOIC ACID < 0. 25 X 0. 25 mg/1 JRN 07/27/00 2117
BENZYL ALCOHOL < 0.050 X o.oso mg/1 JRN 07/27/00 2117
BIS ( 2-CHLOROETHO:-:y) METHANE < 0.050 X 0.050 mg/1 JRN 07/27/00 2117
BIS (2-CHLOROETff£L) ETHER < 0. 050 X 0' 050 mg/1 JRN 07/27/00 2117
BIS(2·CHLOROISOPROPYL)ETHER < 0.050 X 0.050 mg/1 JRN 07/27/00 2117
BIS(2-ETHYLHEXYL)PHTHALATE < 0. 050 X .050 mg/1 JRN 07/27/00 2117
BUTYL BENZYL PHTHALATE < 0.050 X 0.050 mg/1 JRN 07/27/00 2117
CHRYSENE < 0.050 X 0.050 mg/1 JRN 07j27/00 2117
DI-N-BUTYL PHTHALATE < 0 .050 X 0' 050 mg/1 JRN 07/27/00 2117
Dl-N-OCTYI, PHTHALATE < 0.050 X 0.050 mg/1 JRN 07 /27 /00 2117
DIBENZ(A,H)ANTHRACBNB < 0 .050 X 0 .050 mg/1 JRN 07/27/00 2117
DIBBNZOFURAN 0.34 0 .050 mg/1 JRN 07/27/00 2117
DIETHYL PHTHALATB < 0.050 X 0.050 mg/1 JRN 07/27/00 2117
DIMETHYL PHTHALATE < 0.050 X 0.050 mg/1 JRN 07/27/00 2117
FLUORANTHENE < 0.050 X 0. 050 mg/1 JRN 07/27/00 2117
FLUORENE < 0.050 X 0.050 mg/1 JRN 07/27/00 2117
HEXACHLOROBENZENE < 0.050 X 0.050 mg/1 JRN 07/27/00 2117
HEXACHLOROBUTADIENE < 0 .050 X 0' 050 mg/1 JRN 07/27/00 2117
HEXACHLOROCYCLOPENTADIENE < D. 050 X 0.050 mg/1 JRN 07/27/00 2117
HEXACHLOROETHANE < 0.050 X 0, 050 mg/1 JRN 07/27/00 2117
INDENO ( 1, 2, 3 -CD) i'Y~ENE < 0, 050 X 0 .050 mg/1 JRN 07/27/00 2117
ISOPHORONE < 0.050 X 0. 050 mg/1 JRN 07/27/00 2117
N-NITROSODI-N-PP.OPYLAMINE < 0. 050 X 0.050 mg/1 JRN 07/27/00 2117
N·NITROSODIPHENYLAMINE < 0.050 X 0, 050 mg/1 JRN 07/27/00 2117
NAPHTHALBNE 0.71 0.20 mg/1 JRN 07/28/00 1124
NITROBENZENE < 0.050 X 0. 050 mg/1 JRN 07/27/00 2117
PENTACHLOROPHENOL < 0.13 X 0.13 mg/1 JRN 07/27/00 2117
PHENANTHRENE < 0.050 X o. 050 mg/1 JRN 07/27/00 2117
PHENOL o.ose 0 .050 mg/1 JRN 07/27/00 2117
PYRENE < 0. 050 X 0, 050 mg/1 JRN 07/27/00 2117
SW846 8270C DOWT1--IERM
1, l' -BIPHENYL 101 10. 0 mg/1 JRN 07/28/00 1202
BIPHENYL ETHER 292 40.0 mg/1 JRN 07 /31/00 1800
Davis & Floyd, Inc. I PO Drawer 428 1 Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 \ [phone] I Fax [phone]
33
D~S FL D LABORATORY ANALYSIS REPORT
I
Client HNA HOLDINGS INC, Project Number: 61195.00-0003
PO BOX 97
SHELBY, NC 28150 Report. Date Augu:;t. 15, 2000 I
conte\ct ,TERRY MCMURRAY Page 3 of 4
Client ID: F-55 Sample ID L00072D01-08 I
Parameter Result Qual RDL Units Analyst Date Time
Volatile Organics
SW846 8260B I
1,1,1-TRICHLOROETHANE < 0 .0050 0 .0050 mg/1 PAP 07/20/00 1552
1,1,2,2-TETRACHLOROETHANE < o. 0050 0. 0050 mg/1 PAP 07/20/00 1552
1, 1, 2-TRICHLOROETHANE < 0.0050 0 .0050 mg/1 PAP 07/20/00 1552
1, 1-DICHLOROETHANE < 0 . 0050 0 . 0 0 5 0 mg/1 PAP 07 /20/00 1552 I
1,1-DICHLOROETHENE < 0.0050 0 ,0050 mg/1 PAP 07/20/0D 1552
1, 2-DICHLOROETHANE < o.ooso 0 .0050 mg/1 PAP 01/20/00 1552
1,2-DICHLOROPROPANE < 0.0050 0.0050 mg/1 PAP 07/20/00 1552 I
2-BUTANONE 0. 015 0 .010 mg/1 PAP 07/20/00 1552
2-HEXANONE < 0.010 0 . 010 mg/1 PAP 07/20/00 1552
4-METHYL-2-1.'BNTANONE ' 0.0050 0.0050 mg/1 PAP 07/20/00 1552
ACETONE 0.021 0.010 mg/1 PAP 07i20/oo 1552 I
BENZENB 0.054 0 .0050 mg/1 PAP 07/20/00 1552
BROMODICHLOROMETHANE < 0.0050 0.0050 mg/1 PAP 07 /20/00 1552
BROMOFORM < 0 .0050 0.0050 mg/1 PAP 07/20/00 1552
BROMOMBTHANE < 0.010 0. 01.0 mg/1 PAP 07/20/00 1552 I
CARBON DI:3ULFIDE < 0.0050 0 .0050 mg/1 PAP 07/20/00 1.552
CARBON TETRACHLORIDE < 0.0050 0 .0050 mg/1 PAP 07/20/00 1552
CHLOROBENZENE < 0.0050 0.0050 mg/1 PAP 07/20/00 1552
CHLOROETHANE < 0.010 0.010 mg/1 PAP 07/20/00 1552 I
CHLOROFORM < 0.0050 0.0050 mg/1 PAP 07/20/00 1552
CHLOROMETHANE < 0.010 0.010 mg/1 PAP 07/20/00 1552
CIS-1,2-DICHLOROETHGNE < 0.0050 0 .0050 mg/1 PAP 07/20/00 1552
CIS-1,3-DICHLOROPROPENE < 0 .0050 0.0050 mg/1 PAP 07/20/00 1552
I
DI BROMOCHLOROM ETHANE < 0.0050 0 . 0050 mg/1 PAP 07/20/00 1552
ETHYLBENZENE < 0 .0050 0 .0050 mg/1 PAP 07/20/00 1552
METHYLENE CHLORIDE < 0 .0050 0.0050 mg/1 PAP 07/20/00 1552 I
STYRENE < 0.0050 0 .0050 mg/1 PAP 07/20/00 1552
TETRACHLOROETHENE < 0 . 0050 0 . 0050 mg/1 PAP 07/20/00 1552
TOLUENB < 0.0050 0 .0050 mg/1 PAP 07/20/00 1552
TRANS-1, 2-DICHLOROBTHENB < 0.0050 0 .0050 mg/1 PAP 07/20/00 1552 I
TRANS-1, 3 -DICHLOROPROPBNE < 0.0050 0 . 0050 mg/1 PAP 07/20/00 1552
TRICHLOROETHENE < 0.0050 0. 0050 mg/1 PAP 07/20/00 1552
VINYL ACETATB < 0 .010 0 .010 mg/1 PAP 07/20/00 1552 I
VINYL CHLORIDE < 0 .01.0 0.010 mg/1 PAP 07/20/00 1552
XYLENE {TOTAL) < 0.0050 0.0050 mg/1 PAP 07/20/00 1552
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 j 816 E. Durst Avenue
34
\ G,eenwood, SC 29649 \ [phone] \ Fax [phone]
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DAYIS
FLtfi:D LABORATORY ANALYSIS REPORT
Client
C,:,ntact
HNA HOLDINGS INC.
PO BOX 87
.SHELBY, NC 28150
,JERRY MCMURRAY
client ID: 1,-55
Prep Procedure
Analytical Prep Procedures:
BNA SEMIVOLATILES
nowrHERM
Method
SW846 3500B
SWB4.6 35008
Davis & Floyd, lnc. I PO Drawer 428 I Greenwood, SC 29648 I
Project Number: 61195.00-0003
Report Date Augti~t 15, 2000
Page 4 of ,
Sample ID L00072001-0B
Analyst Prep Dato
MCR 07/20/00 1145
MCR 07/20/00 1145
816 E. Durst Avenue
35
I G,eenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLtrYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
PO BOX 87
,SHELBY, NC 28150
JERRY MCMURRAY
Client ID: P-58
Parameter
Field Data
EPA 170.l
TEMPERATURE
SW846 9040B
PH
SWB46 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Orgnnicn
SWB46 8260B
1, 1, !-TRICHLOROETHANE
1,1,2,2-TETRACl!LOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1, 1-DICHLOROETHENE
1, 2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1, 3 -DIC!ILOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1, 2 -DIC!lLOROETHENE
GW/ChemW
Result
20.0
6,4
503
763. 24
< 0.0050
< 0.0050
< 0 .0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.010
< 0.010
< 0.0050
< 0.010
< 0.0050
< 0.0050
0.0050
< 0.010
< 0.0050
< 0.0050
< 0.0050
< 0.010
< 0.0050
< 0.010
< 0.0050
< 0 .0050
< 0 . 0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
Davis & Floyd, lnc. ] PO Drawer 428 I Greenwood, SC 29648 j 816 E. Durst Avenue
36
Project Number: 61195.00-0003
Report Date Augunt 15, 2000
Page l of 2
Sample ID L00072001-09
Date Collected: 19-JUL-OO 13 : 20
Date Received 20-JUL-OO
RDL Units Analyst Date Time
1.0 degrees C 07/19/00 1320
a.so SU 07/19/0D 1320
1.0 umhoo/cm 07/19/00 1320
.01 feet MSL 07/19/00 1320
0.0050 mg/1 PAP 07/20/00 1616
0 .0050 mg/1 PAP 07/20/00 1616
0.0050 mg/1 PAP 07/20/00 1616
0.0050 mg/1 PAP 07/20/00 1616
0.0050 mg/1 PAP 07/20/00 1616
0.0050 mg/1 PAP 07/20/00 1616
0.0050 mg/1 PAP 07/20/00 1616
0. 010 mg/1 PAP 07/20/00 1616
0.010 mg/1 PAP 07/20/00 1616
0.0050 mg/1 PAP 07/20/00 1616
0.010 mg/1 PAP 07/20/00 1616
0.0050 mg/1 PAP 07/20/00 1616
0.0050 mg/1 PAP 07/20/00 1616
0.0050 mg/1 PAP 07 /20";00 1616
0.010 mg/1 PAP 01/20/00 1616
0 .0050 mg/1 PAP 01 /20/00 1616
0.0050 mg/1 PAP 07/20/00 1616
0.0050 mg/1 PAP 07/20/00 1616
0.010 mg/1 PAP 07/20/00 1616
0.0050 mg/1 PAP 07/20/00 1616
0.010 mg/1 PAP 07/20/00 1616
0.0050 mg/1 PAP 07/20/00 1616
0.0050 mg/1 PAP 07/20/00 1616
0 .0050 mg/1 PAP 07/20/00 1616
0 . 0050 mg/1 PAP 01/20/00 1616
0.0050 mg/1 PAP 01/20/00 1616
0.0050 mg/1 PAP 01/20/00 1616
0.0050 mg/1 PAP 07/20/00 1616
0 .0050 mg/1 PAP 01/20/00 1616
0 . 0050 mg/1 PAP 07/20/00 1616
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DAYIS
FL6YD LABORATORY ANALYSIS REPORT
client
(·on tact
HNA HOLDINGS INC.
l'O BOX 87
~HELBY, NC 28150
~lERRY MCMURRAY
Client ID: P-58
Parameter
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
<
<
<
<
<
Project
Report
Page 2
Sample
Ra ii.ult Qual
0.0050
0.0050
0 .010
0.010
0.0050
Number: 61195.00-0003
Date Augu::it 15, 2000
of 2
ID L00072001-09
ROL Units Analyst Date Time
0 .0050 mg/1 PAP 07/20/00 1616
0. 0050 mg/1 PAP 07/20/00 1616
0 .010 mg/1 PAP 07 /20/00 1616
0.010 mg/1 PAP 07/20/00 1616
0.0050 mg/1 PAP 07/20/00 1616
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 1 816 E. Durst Avenue I Greenwood, SC 29649 I (864). 229-4413 I Fax [phone]
37
I
DAYIS
FLMD LABORATORY ANALYSIS REPORT I
Client
Contact
HNA HOLDINGS INC,
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: EE-58
·Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-0ICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
GW/ChemW
Result
18.0
6. 2
72.0
757. 72
< 0. 0050
< 0 . 0050
< 0. 0050
< 0. 0050
< 0 . 0050
< 0 . 0050
0 .0050
< 0.010
< 0. 010
< 0.0050
< 0.010
< 0.0050
< 0.0050
< 0.0050
< 0. 010
< 0. 0050
< 0 .0050
< 0 .0050
< 0.010
< 0.0050
< o. 010
< 0 . 0050
< 0 . 0050
< 0 . 0050
< 0 .0050
< 0. 0050
< 0 . 0050
< 0 . 0050
< 0.0050
< 0.0050
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue
38
I
Project Number: 61195.00-0003
Report Date September 19, 2000
Page 1 of 2 I
Sample ID L00072001-10
Date Collected: 19-JUL-00 14 : 07 I
Date Received 20-JUL-00
Qual RDL Units Analyst Date Time I
1.0 degrees C 07/19/00 1407 I
a.so SU 07/19/00 1407
1. 0 umhos/cm 07/19/00 1407 I
.01 feet MSL 07 /19/00 1407 I
0 .0050 mg/1 PAP 07/20/00 1640
0 .0050 mg/1 PAP 07/20/00 1640
0 .0050 mg/1 PAP 07/20/00 1640 I
0 .0050 mg/1 PAP 07/20/00 1640
0 . 0050 mg/1 PAP 07/20/00 1640
0 . 0050 mg/1 PAP 07/20/00 1640
0.0050 mg/1 PAP 07/20/00 1640
I
0.010 mg/1 PAP 07/20/00 164 0
0.010 mg/1 PAP 07/20/00 1640
0.0050 mg/1 PAP 07/20/00 1640 I
0.010 mg/1 PAP 07/20/00 1640
0.0050 mg/1 PAP 07/20/00 1640
0.0050 mg/1 PAP 07/20/00 1640
0.0050 mg/1 PAP 07/20/00 1640 I
0. 010 mg/1 PAP 07/20/00 164 0
0.0050 mg/1 PAP 07/20/00 1640
0.0050 mg/1 PAP 07/20/00 1640
0.0050 mg/1 PAP 07/20/00 1640 I
0.010 mg/1 PAP 07/20/00 164 0
0.0050 mg/1 PAP 07/20/00 164 0
0.010 mg/1 PAP 07/20/00 164 0 I
0 .0050 mg/1 PAP 07/20/00 1640
o . 0050 mg/1 PAP 07/20/00 1640
0 . 0050 mg/1 PAP 07/20/00 1640
0 .0050 mg/1 PAP 07/20/00 1640 I
0. 0050 mg/1 PAP 07/20/00 164 0
o . 0050 mg/1 PAP 07/20/00 1640
0 . 0050 mg/1 PAP 07/20/00 1640
0 . 0050 mg/1 PAP 07/20/00 1640 I
0.0050 mg/1 PAP 07/20/00 1640
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: EE-58
Parameter
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Result
< 0.0050
< 0.0050
< 0.010
< 0.010
< 0.0050
Project Number:
Report Date
Page 2 of 2
Sample ID
Qual RDL
0 .0050
0.0050
0.010
0.010
0.0050
61195. 00-0003
September 19, 2000
L00072001-10
Units Analyst Date Time
mg/1 PAP 07/20/00 1640
mg/1 PAP 07/20/00 1640
mg/1 PAP 07/20/00 164 0
mg/1 PAP 07 /20/00 1640
mg/1 PAP 07/20/00 1640
Davis & Floyd, Inc. I PO Drawer 428 l Greenwood, SC 29648 I 816 E. Durst Avenue \ Greenwood, SC 29649 I [phone] I Fax [phone]
39
Di\YIS
FLbYD LABORATORY ANALYSIS REPORT
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
SW846 9050
client
contact
Matrix
.SPECIFIC CONDUCTIVITY
GROUND WAT!i:R ELEVATION
Volatile Organics
SW846 826'0B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1, 1-DICHLOROETHANE
1, 1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4 -MBTHYL-2-PENTANONB
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROM OM ETHANE
CARBON DI.'JULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TBTRACHLOKOETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENB
HNA HOLDINas INC.
PO BOY. 87
SP.ELBY, NC 28150
JERRY MCMURRAY
GW/Chem't/
Result
18.0
•••
17.0
842. 71
< 0.0050
< 0.0050
< 0.0050
< o .0050
< o. 0050
< 0.0050
< 0.0050
< 0. 010
< 0.010
< 0.0050
< 0. 010
< 0.0050
< 0.0050
< 0.0050
< 0.010
< 0.0050
< 0.0050
< 0.0050
< 0.010
< 0.0050
< 0.010
< o . 0050
< 0.0050
< o .0050
< 0.0050
< o . 0050
< o . 0050
< 0.0050
< 0.0050
< 0 .0050
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue
40
I
Project Number: 61195.00-0003
I Report Date Auguot 15, 2000
Page 1 of 2
Sample ID L00072001-ll
Date Collected: 19-JUL-OO 15: 36
Date Received 20-JUL-00 I
Qual RDL Units Analyst Date I
1. o degrees C 07/19/00 1536 I
a.so OU 07/19/oo 1536
1.0 umhos/cm 07/19/00 1536 I
. 01 feet MSL 07/19/00 1536
I
0.0050 mg/1 PAP 07/20/00 1752
o .0050 mg/1 PAP 07/20/00 1752
0.0050 mg/1 PAP 07/20/00 1752 I
o ,0050 mg/1 PAP 07/20/00 1752
o. 0050 mg/1 PAP 07 /20/00 1752
0.0050 mg/1 PAP 01/20/00 1752
o .0050 mg/1 PAP 07 /20/00 1752 I
0.010 mg/1 PAP 07/20/00 1752
o .010 mg/1 PAP 07/20/00 1752
0.0050 mg/1 PAP 01/20/00 1752
0. 010 mg/1 PAP 07/20/00 1752 I
0.0050 mg/1 PAP 01/20/00 1752
0.0050 mg/1 PAP 01/20/00 1752
0.0050 mg/1 PAP 07/20/00 1752 I
0.010 mg/1 PAP 07/20/00 1752
0. 0050 mg/1 PAP 07 /20/00 1752
0.0050 mg/1 PAP 07/20/00 1752
0.0050 mg/1 PAP 01/20/00 1752 I
0.010 mg/1 PAP 07/20/00 1752
0.0050 mg/1 PAP 07/20/00 1752
0.010 mg/1 PAP 01/20/00 1752
o .0050 mg/1 PAP 07/20/00 1752 I
0.0050 mg/1 PAP 01/20/00 1752
0.0050 mg/1 PAP 07/20/00 1752
o .0050 mg/1 PAP 01/20/00 1752 I
0.0050 mg/1 PAP 07/20/00 1752
0.0050 mg/1 PAP 07/20/00 1752
o . 0050 mg/1 PAP 07/20/00 1752
o .0050 mg/1 PAP 01/20/00 1752 I
0.0050 mg/1 PAP 07/20/00 1752
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DAYIS
FLtlYD LABORATORY ANALYSIS REPORT
1:1 ient
r:ontact
HNA HOLDINGS INC.
PO BOX 87
:JHELBY, NC 28150
JERRY MCMURRAY
Client ID: C-49
Parameter
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
<
<
' <
<
Project
Report
Page 2
Sample
Result Qual
o.ooso
0.0050
0 . 010
o. 010
0.0050
Number: 61195.00-0003
Date Auguot 15, 2000
of 2
ID L00072001-11
RDL Units Analyst Date Time
0.0050 mg/1 PAP 07/20/00 1752
0.0050 mg/1 PAP 07 /20/00 1752
0 . 010 mg/1 PAP 07/20/00 1752
0.010 mg/1 PAP 07 /20/00 1752
0.0050 mg/1 PAP 07/20/00 1752
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 \ 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
41
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DAYIS
FLtn'D LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
PO BOX 87
.SHELB"{, NC 28150
JERRY MCMURRAY
Client IO: HH-77
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1, 2-DICHLOROETflANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONB
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DI.SULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANB
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHBNB
CIS-1,3-DICHLOROPROPBNB
DIBROMOCHLOROMETHANB
ETHYLBBNZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHBNE
TOLUENE
TRANS-1,2-DICHLOROETHENE
GW/chemW
Result
18.0
s.,
75.0
714. 64
' 0 .0050
' 0.0050
' 0 . 0050
' 0. 0050
' 0. 0050
' 0.0050
' 0.0050
' 0 .010
' 0. 010
' 0.0050
' 0.010
' 0.0050
' 0. 0050
' 0 . 0050
' 0.010
' 0.0050
' 0 .0050
' 0 . 0050
' 0.010
' 0.0050
' 0.010
' 0 .0050
' 0.0050
' 0 ,0050
' 0 .0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
0.0050
Project Number: 61195.00-0003
Report Date Auguot 15, 2000
Page 1 of 2
Sample ID L00072001-12
Date collected: 19-JUL-OO 16 : 32
Date Received 20-JUL-OO
RDL Units Analyst Data Time
1.0 degrees C 07/19/00 1632
0.50 OU 07/19/00 1632
1.0 umhoo/cm 07/19/00 1632
feet MSL 07 /19/00 1632
0. 0050 mg/1 PAP 07/20/00 1816
0.0050 mg/1 PAP 07/20/00 1816
0 .0050 mg/1 PAP 07/20/00 1816
0.0050 mg/1 PAP 07/20/00 1816
o. 0050 mg/1 PAP 07/20/00 1816
0.0050 mg/1 PAP 07/20/00 1816
0.0050 mg/1 PAP 07 /20/00 1816
0.010 mg/1 PAP 07 /20/00 1816
0.010 mg/1 PAP 07/20/00 1816
0.0050 mg/1 PAP 07/20/00 1816
0.010 mg/1 PAP 07/20/00 1816
0 . 0050 mg/1 PAP 07/20/00 1816
0 .0050 mg/1 PAP 07/20/00 1816
0 . 0050 mg/1 PAP 07 /20/00 1816
0. 010 mg/1 PAP 07/20/00 1016
0.0050 mg/1 PAP 07/20/00 1816
0.0050 mg/1 PAP 07 /20/00 1816
o. 0050 mg/1 PAP 07/20/00 1816
0. 010 mg/1 PAP 07/20/00 1816
0.0050 mg/1 PAP 07/20/00 1016
0.010 mg/1 PAP 07/20/00 1816
0.0050 mg/1 PAP 07/20/00 1816
0.0050 mg/1 PAP 07 /20/00 1816
0.0050 mg/1 PAP 07/20/00 1816
0. 0050 mg/1 PAP 07/20/00 1016
0 .0050 mg/1 PAP 07/20/00 1816
0 .0050 mg/1 PAP 07/20/00 1816
0 .0050 mg/1 PAP 07/20/00 1816
0.0050 mg/1 PAP 07 /20/00 1816
0.0050 mg/1 PAP 01 /2 o/oo 1816
Davis & Floyd, Inc. \ PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 \ [phone] l Fax [phone]
42
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DAYIS
FLbYD LABORATORY ANALYSIS REPORT
r:lient
Contact
HNA HOLDINGS INC.
PO BOX :n
.SHELBY, NC 28150
JERRY MCMURRAY
Client ID: HH-77
Parameter
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
'
'
'
'
Project
Report
Page 2
Sample
Result Qual
o.ooso
0 .14
0.010
0.010
0.0050
Number: 61195.00-0003
Date Augu:;t 15, 2000
of 2
ID L00072001-12
RDL Units Analyst Date Time
0. 0050 mg/1 PAP 07/2~/00 1816
0 .0050 mg/1 PAP 07 /20/00 1816
0.010 mg/1 PAP 07/20/00 1816
0.010 mg/1 PAP 07 /2 0/00 1816
0.0050 mg/1 PAP 07/20/00 1816
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 1 [phone] I Fax [phone]
43
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
PO BOX B7
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: HH-48
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
SW846 9050
Mutrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SWB46 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHA.NE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANO~E
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1, 2 -DICHLOROETHENE
GW/ChemW
Result
18.0
5. 3
49.0
714 .11
< 0 . 0050
< 0 .0050
< 0 . 0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.010
< 0.010
< 0.0050
< 0. 010
< o. 0050
< 0.0050
< 0.0050
< 0.010
< 0 .00S0
< 0.0050
< 0 .0050
< 0.010
< 0.0050
< 0.010
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0 .0050
< 0 .00S0
Project Number: 61195.00-0003
Report Date
Page 1 of 2
Sample ID
Augu~t 15, 2000
L00072001-13
Date Collected: 19-JUL-OO 16:35
Date Received 20-JUL-OO
Qual RDL Units Analyst Date Time
1 . 0 degree:J c 07/19/00 1635
a.so SU 07/19/00 1635
1.0 umhos/cm 07/19/00 1635
.01 feet MSL 07/1-9/00 1635
o. 0050 mg/1 PAP 07 /20/00 1840
0 . 0 050 mg/1 PAP 07/20/00 1840
0 .0050 mg/1 PAP 07/20/00 1840
0.0050 mg/1 PAP 07/20/00 1840
0 .0050 mg/1 PAP 07/20/00 1840
0 . 0050 mg/1 PAP 07/20/00 1840
0.0050 mg/1 PAP 07/20/00 1840
0. 010 mg/1 PAP 07/20/00 1840
0.010 mg/1 PAP 07/20/00 1840
0.0050 mg/1 PAP 07/20/00 1840
0.010 mg/1 PAP 07/20/00 1840
0.0050 mg/1 PAP 07/20/00 1840
o.ooso mg/1 PAP 07/20/00 1840
0.0050 mg /1 PAP 07/20/00 1840
0.010 mg/1 PAP 07/20/00 1840
0 . 0050 mg/1 PAP 07/20/00 1840
0.0050 mg/1 PAP 07 /20/00 1840
0.0050 mg/1 PAP 07/20/00 1840
0.010 mg/1 PAP 07/20/00 1840
0.0050 mg/1 PAP 07/20/00 1840
0.010 mg/1 PAP 07/20/00 1840
o.ooso mg/1 PAP 07/20/00 1840
0.0050 mg/1 PAP 07/20/00 1840
0.0050 mg/1 PAP 07/20/00 1840
0. 0050 mg/1 PAP 07/20/00 1840
0 .0050 mg/1 PAP 07/20/00 1840
0.0050 mg/1 PAP 07/20/00 1840
0.0050 mg/1 PAP 07/20/00 1840
0.0050 mg/1 PAP 07/20/00 1840
0 .0050 mg/1 PAP 07/20/00 1840
Davis & Floyd, Inc. \ PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue \ Greenwood, SC 29649 \ [phone] I Fax [phone]
44
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Df\VIS
FLlfYD LABORATORY ANALYSIS REPORT
client
Contact
HNA HOLDINGS INC.
PO BOX 87
.SHELBY, NC 28150
JERRY MCMURRAY
client ID: HH-48
Parameter
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACBTATE
VINYL CHLORIDE
XYLENE: (TOTAL)
Result
0.0050
0.072
< 0.010
0 .010
< 0.0050
Project Number:
Report Date
Page 2 of 2
Sample ID
Qual RDL
0. 0050
0.0050
0. 010
o. 010
0.0050
61195. 00-0003
Augunt 15, 2000
L00072001-13
Units Analyst Date Time
mg/1 PAP 01/20/00 1840
mg/1 PAP 01/20/00 1840
mg/1 PAP 01/20/00 1840
mg/1 PAP 07/20/00 1840
mg/1 PAP 01/20/00 1840
Davis & Floyd, Inc. I PO Drawer 428 ! Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
45
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DAYIS
FLt1\'D LABORATORY ANALYSIS REPORT
client
(:on tact
HNA HOLDINGS INC,
PO BOX S7
SHELBY, NC 28150
,TERRY MCMURRAY
1:•lient ID: T-35
Parameter
Field Data
EPA 170.l
TEMPERATURE
SW846 9040B
PH
SW846 9050
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETJlANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL 2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICJ-ILOROETHENE
GW/Cht;mW
Result
19 .o
5,2
449
765 .12
< 0 .0050
< 0.0050
< 0 .0050
< 0 .0050
< 0 .0050
< 0 .0050
< 0. 0050
< 0.010
< 0. 01.0
< 0.0050
< 0.010
< 0.0050
< 0 . 0050
< 0 . 0050
< 0.010
< 0 .0050
< 0.0050
< 0 . 0050
< 0. 010
< 0.0050
< 0.010
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0,0050
< 0 .0050
0.0050
Project Number: 61195.00-0003
Report Date Augw::it 15, 2000
Page 1 of 2
Sample ID L0007200l-14
Date Collected: 19-JUL-OO 17 : 30
Date Received 20-JUL-00
Qual RDL Units Analyst Date Time
1. 0 degreen c 07/19/00 1730
a.so OU 07/19/00 1730
1 . 0 umhoo/cm 07/19/00 1730
. 01 feet MSL 07/1-9/00 1730
0.0050 mg/1 PAP 07/20/00 1904
0 . 0050 mg/1 PAP 01/20/00 1904
0.0050 mg/1 PAP 07/20/00 1904
0 .0050 mg/1 PAP 07/20/00 1904
0 .0050 mg/1 PAP 07/20/00 1904
0.0050 mg/1 PAP 07/20/00 1904
0.0050 mg/1 PAP 07/20/00 1904
0 .010 mg/1 PAP 07/20/00 1904
0.010 mg/1 PAP 07/20/00 1.904
0.0050 mg/1 PAP 07/20/00 1904
0.010 mg/1 PAP 07/20/00 1904
0 .0050 mg/1 PAP 07/20/00 1904
0 .0050 mg/1 PAP 07/20/00 1904
0.0050 mg/1 PAP 07/20/00 1904
0. 010 mg/1 PAP 07/20/00 1904
0 .0050 mg/1 PAP 01/20/00 1.904
0.0050 mg/1 PAP 07/20/00 1904
0 .0050 mg/1 PAP 07/20/00 1904
0.010 mg/1 PAP 07/20/00 1904
0.0050 mg/1 PAP 07/20/00 1904
0.010 mg/1 PAP 07/20/00 1904
o. 0050 mg/1 PAP 01/20/00 1904
0.0050 mg/1 PAP 07 /20/00 1904
0.0050 mg/1 PAP 07/20/00 1904
0.0050 mg/1 PAP 07/20/00 1904
0.0050 mg/1 PAP 07/20/00 1904
0.0050 mg/1 PAP 07/20/00 1904
0 . 00 so mg/1 PAP 07/20/00 1904
0.0050 mg/1 PAP 07/20/00 1904
0 .0050 mg/1 PAP 07/20/00 1904
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
46
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DAYIS
FLtwD LABORATORY ANALYSIS REPORT
client
Contact:
HNA HOLDINGS INC,
PO BOY. 87
,':HlELBY, NC 28150
JERRY MCMURRAY
client ID: T-35
Parameter
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACET:"',TE
VINYL CHLORIDE
XYLENE (TOTAL)
<
<
<
<
<
Project
Report
Page 2
Sample
Result Qual
o. 0050
0.0050
0 .010
0 .010
0.0050
Number: 61195.00-0003
Date Auguot 15, 2000
of 2
ID L00072001-14
RDL Units Analyst Date Time
0.0050 mg/1 PAP 07 /20/00 1904
0 .0050 mg/1 PAP 07/20/00 1904
0 .010 mg/1 PAP 07/20/00 1904
0.010 mg/1 PAP 07/20/00 1904
0.0050 mg/1 PAP 07/20/00 1904
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 j 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] \ Fax [phone]
47
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Di\VIS
FLtrYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
PO BOX 37
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: FF-34
Parameter
Field Data
SPA 170.1
TEMPERATURE
SW846 9040B
PH
SW846 9050
11;,,tr.i.x
SPECIFIC CONDUCTIVITY
GROUND WATER ELEilATION
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1, 1 -DICHLOROETHP_NE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1, 2 -DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENF. CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
GW/ChemW
Raault
17.0
5 .1
49.0
760.47
< 0.0050
0 . 0050
< 0. 0050
0.0050
< 0 .0050
< 0.0050
< 0.0050
< 0.010
< 0. 010
< 0.0050
< 0.010
< 0.0050
< 0 . 0050
< 0 . 0050
< 0.010
< 0 . 0050
< o. 0050
< 0.0050
< 0.010
< 0.0050
< 0.010
< 0.0050
< 0.0050
0. 0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
Project Number: 61195.00-0003
Report Date Auguat 15, 2000
Page 1 of 2
Sample ID L00072001-15
Date Collected: 19-JUL-00 18: 25
Date Received 20-JUL-00
Qual RDL Units Analyst Date Time
1.0 degreeo c 07/19/00 1825
0.50 SU 07/19/00 1825
1. 0 umhori/cm 07/19/00 1825
.01 feet MSL 07/19/00 1825
0.0050 mg/1 PAP 07/20/00 1!,28
0 .0050 mg/1 PAP 07/20/00 1928
0 .0050 mg/1 PAP 07/20/00 1928
0.0050 mg/1 PAP 07/20/00 1928
0. 0050 mg/1 PAP 07/20/00 1928
0.0050 mg/1 PAP 07 /2 o/oo 1928
0 .0050 mg/1 PAP 07/20/00 1928
0.010 mg/1 PAP 07/20/00 1928
0 .010 mg/1 PAP 07/20/00 1928
0.0050 mg/1 PAP 07 /20/00 1928
0.010 mg/1 PAP 07/20/00 1928
0 .0050 mg/1 PAP 07/20/00 1928
0.0050 mg/1 PAP 07/20/00 1928
0.0050 mg/1 PAP 07/20/00 1928
0.010 mg/1 PAP 07/20/00 1928
0 . 0050 mg/1 PAP 07/20/00 1928
0.0050 mg/1 PAP 07/20/00 1928
0.0050 mg/1 PAP 07 /20/00 1928
0.010 mg/1 PAP 07/20/00 1928
0.0050 mg/1 PAP 07/20/00 1928
0.010 mg/1 PAP 07/20/00 1928
0 .0050 mg/1 PAP 07/20/00 1928
0.0050 mg/1 PAP 07/20/00 1928
0. 0050 mg/1 PAP 07/20/00 1928
0 .0050 mg/1 PAP 07/20/00 1928
0 .0050 mg/1 PAP 07/20/00 1928
0.0050 mg/1 PAP 07 /20/00 1928
0 ,0050 mg/1 PAP 07/20/00 1928
0 . 0050 mg/1 PAP 07/20/00 1928
0 .0050 mg/1 PAP 07/20/00 1928
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue j Greenwood, SC 29649 j [phone] I Fax [phone]
48
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Df\YIS
FLtfYD LABORATORY ANALYSIS REPORT
Client.
Cunt act
HNA HOLDINOS INC.
PO BOX 87
.SHELEY, NC 28150
,TERRY 1·'.CMURRAY
Client ID: FF-34
Parameter
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL l
Result
' 0 . 0050
' 0.0050
' 0.010
' 0.010
' 0.0050
Project Number:
Report Date
Page 2 of 2
Sample ID
Qual RDL
0.0050
0.0050
0.010
0 .010
0.0050
61195. 00-0003
Auguat 15, 2000
L00072001-15
Units Analyst Date Time
mg/1 PAP 07/20/00 1928
mg/1 PAP 07/20/00 1928
mg/1 PAP 01/20/00 1928
mg/1 PAP 01/20/00 1928
mg/1 PAP 07/20/00 1928
Davis & Floyd, Inc. I PO Drawer 428 \ Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
49
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DAYIS
FLtfYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
PO BOX Si
.SHELBY, Ne 28150
JERRY MCMURRAY
client ID: FF-62
Parameter
Field Data
EPA 170.1
TEMPERATURE
SWB46 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SWB46 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONB
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DI.'.>ULFIOE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENB
CIS-1,3-0ICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TBTRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
GW/ChemW
Result
18.0
5.7
61,0
759.78
< 0 .0050
< 0 .0050
< 0. 0050
< 0 .0050
< 0.0050·
< 0.0050
< 0.0050
< 0.010
< 0.010
< 0.0050
< 0.010
< 0.0050
< 0.0050
< 0.0050
< 0.010
< 0.0050
< 0.0050
< 0.0050
< 0.010
< 0.0050
< 0.010
< 0 .0050
< 0 .0050
< 0.0050
< 0.0050
0.0050
< 0 .0050
< 0.0050
< o.0050
< 0.0050
Project Number: 61195.00-0003
Report Date
Page 1 of 2
Sample ID
Augunt 15, 2000
L00072001-16
Date Collected: 19-JUL-OO 18:35
Date Received 20-JUL-OO
Qual RDL Units Analyst Date Tima
l.O degreen C 07/19/00 1835
a.so nu 07/19/00 1835
1.0 umhon/cm 07/19/00 1835
. 01 feet MSL 07/19/00 1835
0. 0050 mg/1 PAP 07/20/00 1952
0 .0050 mg/1 PAP 07/20/00 1952
0 .0050 mg/1 PAP 07/20/00 1952
0 ,0050 mg/1 PAP 01/20/00 1952
0.0050 mg/1 PAP 07/20/00 1952
0.0050 mg/1 PAP 07/20/00 1952
0.0050 mg/1 PAP 07/20/00 1952
0.010 mg/1 PAP 07/20/00 1952
0 .010 mg/1 PAP 01/20/00 1952
0.0050 mg/1 PAP 07/20/00 1952
0.010 mg/1 PAP 07/20/00 1952
0.0050 mg/1 PAP 07/20/00 1952
0. 0050 mg/1 PAP 07 /20/00 1952
0 .0050 mg/1 PAP 07/20/00 1952
0.010 mg/1 PAP 07/20/00 1952
0.0050 mg/1 PAP 01/20/00 1952
0 .0050 mg/1 -PAP 01/20/00 1952
0.0050 mg/1 PAP 07/20/00 1952
0.010 mg/1 PAP 07/20/00 1952
0.0050 mg/1 PAP 01/20/00 1952
0. 010 mg/1 PAP 07 /20/00 1952
0.0050 mg/1 PAP 07/20/00 1952
0.0050 mg/1 PAP 07/20/00 1952
0.0050 mg/1 PAP 07/20/00 1952
0 .0050 mg/1 PAP 07/20/00 1952
0.0050 mg/1 PAP 07/20/00 1952
0 .0050 mg/1 PAP 01/20/00 1952
0.0050 mg/1 PAP 01/20/00 1952
0. 0050 mg/1 PAP 07/20/00 1952
0 .0050 mg/1 PAP 01/20/00 1952
Davis & Floyd, Inc. I PO Drawer 428 \ Greenwood, SC 29648 ] 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] 1 Fax [phone]
50
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
C"',::,ntact
RNA HOLDINGS INC.
PO BOX 87
.'JHELBY, NC 28150
JERRY MCMURRAY
client ID: FF-62
Parameter
TRANS-1,3-DICHLOROPROPENE
TRICHI.,OROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Reault
' 0 . 0050
' 0. 0050
< 0.010
' 0. 010
< 0.0050
Project Number: 61195. 00-0003
Report Date Augunt 15, 2000
Page 2 of 2
Sample ID L00072001-16
Qual RDL Units Analyst Date Time
0 .0050 mg/1 PAP 07 /20/00 1952
0 .ooso mg/1 PAP 07/20/00 1952
0.010 mg/1 PAP 07/20/00 1952
0. 010 mg/1 PAP 07/20/00 1952
0.0050 mg/1 PAP 07/20/00 1952
Davis & Floyd, Jnc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] j Fax [phone]
51
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D1\VIS
FLOYD LABORATORY ANALYSIS REPORT
Client
r;ontact
HNA HOLDINGS INC.
PO BOX 87
;:;Hl,LBY, NC 28150
,TERRY MCMURRAY
(;lient ID: GG-61
Parameter
Field Data
EPA 170.l
TBMPERATURE
SW846 9040B
PH
SWB46 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROF.THENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-MBTHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHBNE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1, 2-DICHLOROETHENE
GW/ChemW
Result
17. 0
6.1
96.0
751.96
' 0.0050
' 0 .0050
' 0.0050
' 0.0050
' 0.0050
' 0 . 0050
' 0.0050
' 0.010
' 0.010
' 0.0050
' 0.010
' 0.0050
' 0.0050
' 0.0050
' 0,010
' 0.0050
' 0.0050
' o.ooso
' 0.010
' 0.0050
' 0.010
' 0. 0050
' 0 . 0050
' 0.0050
' 0 .ooso
' 0. 0050
' o.ooso
' 0.0050
' 0.0050
' 0.0050
Project Number: 61195.00-0003
Report Date Auguat 15, 20 00
Page 1 of 2
Sample ID L00072001-17
Date Collected: 19-JUL-OO 19 : JS
Date Received 20-JUL-OO
Qual RDL Units Analyst Data Time
1. 0 degreeo c 07/19/00 1935
0.50 OU 07/19/00 1935
1. 0 umhoo/cm 07 /19/00 1935
.01 feet MSL 07/19/00 1935
0.0050 mg/1 PAP 07/20/00 2016
.0050 mg/1 PAP 07/20/00 2016
0.0050 mg/1 PAP 07/20/00 2016
0. 00 so mg/1 PAP 07/20/00 2016
0.0050 mg/1 PAP 07/20/00 2016
0 .0050 mg/1 PAP 07/20/00 2016
0.0050 mg/1 PAP 01/20/00 2016
o. 010 mg/1 PAP 07 /20/00 2016
0.010 mg/1 PAP 07/20/00 2016
0.0050 mg/1 PAP 07/20/00 2016
0.010 mg/1 PAP 07/20/00 2016
0 .0050 mg/1 PAP 07/20/00 2016
0 .ooso mg/1 PAP 07/20/00 2016
0 .0050 mg/1 PAP 07/20/00 2016
0. 010 mg/1 PAP 07/20/00 2016
0.0050 mg/1 PAP 07/20/00 2016
0.0050 mg/1 PAP 07 /20/00 2016
0.0050 mg/1 PAP 07/20/00 2016
0. 010 mg/1 PAP 07/20/00 2016
0.0050 mg/1 PAP 07/20/00 2016
0.010 mg/1 PAP 07/20/00 2016
0 . 0050 mg/1 PAP 07/20/00 2016
0 .ooso mg/1 PAP 07/20/00 2016
0 . 00 so mg/1 PAP 07/20/0D 2016
0 .0050 mg/1 PAP 07 /20/00 2016
0.0050 mg/1 PAP 07/20/00 2016
0 . 0050 mg/1 PAP 07/20/00 2016
0 .0050 mg/1 PAP 07/20/00 2016
0 .0050 mg/1 PAP 07/20/00 2016
0 .ooso mg/1 PAP 07 /20/00 2016
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 Es~rst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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DAYIS
FLtfYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDIUGS INC.
PO BOX 87
.SHELBY, NC 28150
JERRY MCMURRAY
Cli~nt ID: GG-61
Parameter
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYI, ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Result
< 0.0050
< 0 .0050
< 0.010
< 0.010
< 0.0050
Project Number:
Report Date
Page 2 of 2
Sample ID
Qual RDL
0. 0050
0 .0050
0. 010
0 .010
0.0050
61195.00-0003
Augunt 15, 2000
L00072001-17
Units Analyst Date Time
mg/1 PAP 07/20/00 2016
mg/1 PAP 07/20/00 2016
mg/1 PAP 07/20/00 201.6
mg/1 PAP 07/20/00 2016
mg/1 PAP 07/20/00 2016
Davis & Floyd, Inc. I PO Drawer 428 \ Greenwood, SC 29648 I 816 Es 3urst Avenue I Greenwood, SC 29649 I [phone] I Fax {864) 229-7119
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DAYIS
FLtfYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: GG-61 DUP.
Pa:ramoter
Field Data
EPA 170.l
TEMPERATURE
SW846 904GB
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL 2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENB
DIBROMOCHLOROMET!-\ANB
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TBTRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
GW/ChemW
Result
17.0
6.1
96,0
751.96
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.010
< 0.010
< 0.0050
< 0.010
< 0.0050
< 0.0050
< 0 .0050
< 0.010
< 0.0050
< 0 . 0050
< 0.0050
< 0. 010
< 0.0050
< 0.010
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0 .ooso
< 0.0050
< 0.0050
< 0.0050
< 0.0050
Project Number: 61195.00-0003
Report Date Auguot. 15, 2000
Page 1 of 2
Sample ID L000720D1-18
Date Collected: 19-JOL-OO 19: 3 S
Date Received 20-JUL-OO
Qual RDL Units Analyst Date Time
1. 0 degrees C 07/19/00 1935
0.50 07/19/00 1935
1. 0 umhm1/cm 07/19/00 1935
.01 feet MSL 07/19/00 1935
0.0050 mg/1 PAP 07/20/00 2040
0.0050 mg/1 PAP 07 /20/00 2040
0 .0050 mg/1 PAP 07/20/00 2040
0 . 0050 mg/1 PAP 07/20/00 2040
0.0050 mg/1 PAP 07 /20/00 2040
0. 0050 mg/1 PAP 07/20/00 2040
0. 0050 mg/1 PAP 07/20/00 2040
0 .010 mg/1 PAP 07/20/00 2040
0.010 mg/1 PAP 07/20/00 2040
0,0050 mg/1 PAP 07/20/00 2040
0. 010 mg/1 PAP 01 /2 o/oo 2040
0.0050 mg/1 PAP 07/20/00 2040
0.0050 mg/1 PAP 07/20/00 2040
0.0050 mg/1 PAP 07/20/00 2040
0.010 mg/1 PAP 07/20/00 2040
0. 0050 mg/1 PAP 07/20/00 2040
0.0050 mg/1 PAP 07 /20/00 2040
0.0050 mg/1 PAP 07/20/00 2040
0.010 mg/1 PAP 07/20/00 2040
0.0050 mg/1 PAP 07/20/00 2040
0.010 mg/1 PAP 07/20/00 2040
0 .0050 mg/1 PAP 07/20/00 2040
0.0050 mg/1 PAP 07/20/00 2040
0.0050 mg/1 PAP 07/20/00 2040
0 .0050 mg/1 PAP 07/20/00 2040
0.0050 mg/1 PAP 01/20/00 2040
0 .0050 mg/1 PAP 07/20/00 2040
0 .0050 mg/1 PAP 07/20/00 2040
0 .0050 mg/1 PAP 07/20/00 2040
o.ooso mg/1 PAP 07/20/00 2040
Davis & Floyd, Inc. I PO Drawer 428 \ Greenwood, SC 29648 \ 816 E. Durst Avenue \ Greenwood, SC 29649 I {864) 229-4413 I Fax [phone]
54
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DAYIS
FLtfYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
PO EOX 87
.SHELBY, NC 28150
cTERRY MCMURRAY
Cli.ent ID: GG-61 oup,
Parameter
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Result
< 0.0050
< 0.0050
< 0.010
< 0.010
< 0.0050
Project Number:
Report Date
Page 2 of 2
Sample ID
Qual RDL
0.0050
0.0050
o. 010
0.010
0.0050
61195.00-0003
Auguot: 15, 2000
L0007200l-18
Units Analyst Date Time
mg/1 PAP 07 /20/00 2040
mg/1 PAP 07/20/00 2040
mg/1 PAP 07/20/00 2040
mg/1 PAP 07/20/00 2040
mg/1 PAP 07/20/00 2040
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E.SDSrst Avenue j Greenwood, SC 29649 I {864) 229-4413 I Fax [phone]
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DAYIS
FLt1YD LABORATORY ANALYSIS REPORT
Client
Cont'-'ct
HNA HOLDINGS INC.
PO BOX 87
.'.lHELBY, NC: 28150
JERRY MCl1URRAY
Client ID: AA-54
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
SWB46 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SW846 826GB
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRIC!!LOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-0ICHLOROPROPAN8
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIG-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
GW/Chem/V
Result
16.0
4.7
280
746.90
< 0. 0050
< 0. 0050
< 0.0050
< 0 . 0050
< 0.0050
o.ooso
< 0.0050
< 0 . 010
< 0 . 010
< 0.0050
< 0.010
< 0.0050
< 0.0050
< o.ooso
0. 010
< 0.0050
< o.ooso
< 0.0050
0. 010
0.0050
< 0.010
o.ooso
< 0.0050
< 0.0050
< 0.0050
< 0 .ooso
< 0.0050
< 0.0050
< 0.0050
< 0.0050
Project Number: 61195.00-0003
Report Date Augu::it 15, 2000
Page l of 2
Sample ID L00072D01-19
Date Collected: 19-JUL-OO 20: OB
Date Received 20-JUL-OO
Qual RDL Time
1.0 degreeo C 07/19/00 2008
0.50 07/19/00 2008
1.0 umhon/cm 07/19/00 2008
feet MSL 07/19/00 2008
0.0050 mg/1 PAP 07/21/00 091B
0 .0050 mg/1 PAP 07/21/00 091B
0.0050 mg/1 PAP 07/21/00 0918
0 .0050 mg/1 PAP 07 /21/00 0918
0 .0050 mg/1 PAP 07/21/00 091B
0.0050 mg/1 PAP 07/21/00 0918
0.0050 mg/1 PAP 07/21/00 0918
0 . 010 mg/1 PAP 07/21/00 0918
0 . 010 mg/1 PAP 07/21/00 0918
0.0050 mg/1 PAP 07/21/00 091B
0.010 mg/1 PAP 07/21/00 0918
0.0050 mg/1 PAP 07/21/00 0918
0.0050 mg/1 PAP 07/21/00 0918
0 .0050 mg/1 PAP 07/21/00 0918
0.010 mg/1 PAP 07/21/00 0918
0.0050 mg/1 PAP 07/21/00 0918
0 .ooso mg/1 PAP 07/21/00 0918
0.0050 mg/1 PAP 07/21/00 0918
0.010 mg/1 PAP 07/21/00 091B
0.0050 mg/1 PAP 07/21/00 0918
0.010 mg/1 PAP 07/21/00 0918
0.0050 mg/1 PAP 07/21/00 0918
0.0050 mg/1 PAP 07 /21/00 0918
0 ,0050 mg/1 PAP 07/21/00 0918
0 . 0050 mg/1 PAP 07/21/00 0918
0. 0050 mg/1 PAP 07/21/00 0918
0 .0050 mg/1 PAP 07 /21/00 0918
0 . 0050 mg/1 PAP 07 /21/00 0918
0 .0050 mg/1 PAP 07/21/00 0918
0. 0050 mg/1 PAP 07/21/00 0918
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue l Greenwood, SC 29649 I {864) 229-4413 I Fax [phone]
56
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DAYIS
FLtiYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINOS INC.
PO BOX 87
5H8LBY, NC 28150
JEP.RY MCMURRAY
Client ID: AA-54
Parameter
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLBNE (TOTAL)
Result
o. 0050
< 0. 0050
< o. 010
< 0 .010
< 0.0050
Project Number: 61195 .00-0003
Report Date Augu.st 15, 2000
Page 2 of 2
Sample ID L00072001-19
Qual RDL Uni ta Analyat Date Time
0 .0050 mg/1 PAP 07/21/00 0918
0.0050 mg/1 PAP 07 /21/00 0918
0.010 mg/1 PAP 07/21/00 0918
0. 010 mg/1 PAP 07 /21/00 0918
0.0050 mg/1 PAP 07/21/00 0918
Davis & Floyd, Inc. j PO Drawer 428 \ Greenwood, SC 29648 I Bl 6 E. Durst Avenue I Greenwood, SC 29649 I {864) 229-4413 l Fax [phone]
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DAYIS
FLt1YD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
PO BOX 87
SHELBY, NC 20150
JERRY MCMURRAY
Client ID: K-28
Parameter
Field Data
EPA 170.1
TEMPERATURE
SWB46 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANB
CARBON DISULFIDE
CARBON TBTRACHLORIDE
CHLOROBENZENE
CHLOROETHANB
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHBNE
CIS-1,J-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENB
GW/ChemW
Result
18.0
,.1
250
789. 94
< 0. 0050
< 0 .0050
< 0. 0050
< 0 .0050
< 0.0050
< 0.0050
< 0.0050
< 0.010
< 0.010
< 0.0050
< 0. 010
0.010
< 0.0050
< 0 .0050
< 0.010
< 0.0050
< 0.0050
< 0.0050
< 0.010
< 0.0050
< 0.010
< 0 .0050
< 0 .0050
< 0.0050
< 0.0050
< 0 .0050
< 0 . 0050
< o. 0050
< 0.0050
< 0.0050
Project Number: 61195.00-0003
Report Date
Page 1 of 2
Sample ID
August 15, 2000
L00072001-20
Date Collected: 19-JUL-00 20:20
Date Received 20-JUL-OO
Qual RDL Units P.nalyat Date Time
1. 0 degrees C 07/19/00 2020
0.50 ,u 07/19/0D 2020
1.0 umhoo/cm 07/19/00 2020
.01 feet MSL 07/19/00 2020
o. 0050 mg/1 PAP 07 /21/00 1030
0.0050 mg/1 PAP 07/21/00 1030
0 .0050 mg/1 PAP 07 /21/00 1030
0.0050 mg/1 PAP 07/21/00 1030
0.0050 mg/1 PAP 07/21/00 1030
0.0050 mg/1 PAP 07 /21/00 1030
0.0050 mg/1 PAP 07/21/00 1030
0.010 mg/1 PAP 07/21/00 1030
0.010 mg/1 PAP 07/21/00 1030
0.0050 mg/1 PAP 07/21/00 1030
0.010 mg/1 PAP 07/21/00 1030
0.0050 mg/1 PAP 07/21/00 1030
0.0050 mg/1 PAP 07/21/00 1030
0.0050 mg/1 PAP 07/21/00 1030
0.010 mg/1 PAP 07/21/00 1030
0 .0050 mg/1 PAP 07/21/00 1030
0. 0050 mg/1 PAP 07/21/00 1030
o.ooso mg/1 PAP 07/21/00 1030
0.010 mg/1 PAP 07 /21/00 1030
0.0050 mg/1 PAP 07/21/00 1030
0.010 mg/1 PAP 07 /21/00 1030
0 .0050 mg/1 PAP 07 /21/00 1030
0 .0050 mg/1 PAP 07 /21/00 1030
0.0050 mg/1 PAP 07/21/00 1030
0.0050 mg/1 PAP 07/21/00 1030
o. 0050 mg/1 PAP 07/21/00 1030
0.0050 mg/1 PAP 07/21/00 1030
0.0050 mg/1 PAP 07/21/00 1030
0 .0050 mg/1 PAP 07/21/00 1030
0.0050 mg/1 PAP 07/21/00 1030
Davis & Floyd, Inc. I PO Drawer 428 j Greenwood, SC 29648 I Bl 6 E. Durst Avenue I Greenwood, SC 29649 \ [phone] l Fax [phone]
58
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D1\YIS
FLt1YD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
PO BOX 87
.SHELBY, NC 28150
JERRY MCMURRAY
r:1ient ID: K-28
Parameter
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Wet Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
Result
' 0 .0050
' 0 .0050
' 0.010
' 0.010
' o.ooso
16.7
Project Number: 61195. 00-0003
Report Date Auguot 15, 2000
Page 2 of 2
Sample ID L00072001-20
Qual RDL Units Analyst Date Time
0. 0050 mg/1 PAP 07/21/00 1030
0.0050 mg/1 PAP 07/21/00 1030
0.010 mg/1 PAP 07/21/00 1030
0.010 mg/1 PAP 07/21/00 1030
0.0050 mg/1 PAP 07/21/00 1030
1.0 mg/1 TRB 07/27/00 1330
Davis & Floyd, Inc. I PO Drawer 428 j Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] l Fax [phone]
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D!\YIS
FLMD LABORATORY ANALYSIS REPORT
client
Contact
HNA HOLDINGS INC.
PO BOX 87
.SHELBY, NC 28150
JERRY MCMURRAY
Client ID: V-23
Parameter
Field Data
EPA 170.l
TEMPERATURE
SW846 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL 2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHAN"E
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
GW/ChemW
Result
18.0
s.o
5910
794.45
< 0.015
< 0 .015
< 0.015
< 0 .015
< o. 015
< 0. 015
< 0.015
0.42
< 0.030
< 0.015
0.47
0.021
< 0.015
< 0.015
< 0.030
0.041
< 0.015
< 0.015
< 0.030
< 0. 015
< 0.030
0.015
< 0 .015
< 0.015
< 0.015
< 0.015
< 0.015
< 0.015
< 0.015
< o. 015
Project Number: 61195.00-0003
Report Date
Page 1 of 2
Sample ID
Date Collected:
Date Received
Qual RDL
1.0
0.50
1.0
. 01
X 0 .015
X 0.015
X 0. 015
X 0.015
X 0.015
X 0 .015
X 0. 015
0.030
X 0.030
X 0 .015
0.030
0.015
X 0 .015
X 0.015
X 0.030
0.015
X 0 .015
X 0 .015
X 0.030
X 0. 015
X o. 030
X 0. 015
X 0.015
X 0 .015
X 0 .015
Y. 0.015
X 0.015
X 0. 015
X 0 .015
X 0.015
Auguct 15, 2000
L00072001-21
19-JUL-OO 20:45
20-JUL-OO
Units Analyst Date Time
degreeo C 07/19/00 2045
SU 07/19/00 2045
umhon/cm 07/19/00 2045
feet MSL 07/19/00 2045
mg/1 PAP 07 /21/00 1657
mg/1 PAP 07/21/00 1657
mg/1 PAP 07/21/00 1657
mg/1 PAP 07/21/00 1657
mg/1 PAP 07/21/00 1657
mg/1 PAP 07/21/00 1657
mg/1 PAP 07/21/00 1657
mg/1 PAP 07 /21/00 1657
mg/1 PAP 07 /21/00 1657
mg/1 PAP 07/21/00 1657
mg/1 PAP 01/21/00 1657
mg/1 PAP 07/21/00 1657
mg/1 PAP 07 /21/00 1657
mg/1 PAP 07/21/00 1657
mg/1 PAP 07 /21/00 1657
mg/1 PAP 07/21/00 1657
mg/1 PAP 07 /21/00 1657
mg/1 PAP 07 /21/00 1657
mg/1 PAP 07/21/00 1657
mg/1 PAP 07 /21/00 1657
mg/1 PAP 07/21/00 1657
mg/1 PAP 07 /21/00 1657
mg/1 PAP 07/21/00 1657
mg/1 PAP 07/21/00 1657
mg/1 PAP 07/21/00 1657
mg/1 PAP 07 /21/00 1657
mg/1 PAP 07/21/00 1657
mg/1 PAP 07/21/00 1657
mg/1 PAP 07/21/00 1657
mg/1 PAP 07 /21/00 1657
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 \ 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
60
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DAYIS
FLtJ\'D LABORATORY ANALYSIS REPORT
Client
Cont,.3.ct
HNA HOLDINGS INC.
PO BOX 87
.SHELEY, NC 28150
JERRY MCMURRAY
client ID: V-23
Parameter
TRANS-!, 3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Wot Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
'
'
'
'
Project
Report
Page 2
.Sample
Result Qual
0 . 015 X
0 -015 X
0. 030 X
0 . 030 X
0.015 X
11700
Number: 61195.00-0003
Date August 15, 2000
of 2
ID L00072001-21
RDL units Analyst Date Time
0 .015 mg/1 PAP 07/21/00 1657
0 .015 mg/1 PAP 07/21/00 1657
0 .030 mg/1 PAP 07/21/00 1657
0.030 mg/1 PAP 07/21/00 1657
0.015 mg/1 PAP 07/21/00 1657
20.0 mg/1 TRB 07/27/00 1421
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 EBDfrst Avenue I Greenwood, SC 29649 l [phone] I Fax (864} 229-7119
DAYIS
FLMD LABORATORY ANALYSIS REPORT
:--~on tact
HNA HOLDINGS INC,
PO BOX 87
.'1HELBY, NC 28150
JERRY MCMURRAY
client ID; FIELD BLANK
tle,trix
Parameter
Volatile Organics
SW846 82G0B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1, 1, 2 -TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-!lEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLORO!·lETHANE
BROMOFORM
BROMOMETHANB
CARBON DI.SULFIDF.:
CARBON TETRACHLORIDE
CHLOROBENZENB
CHLOROETHANE
CHLOROFORM
CHLOROMSTHANS
CIS-1,2-DICHLOROETHSNS
CIS-1,3-DICHLOROPROPENS
DIBROMOCHLOROMETHANB
BTHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TSTRACHLOROETHENE
TOLUENS
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLSNE (TOTAL)
GW/Ch~mw
Result
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0. 0050
< 0 .0050
< 0.0050
< 0.010
< 0.010
< 0.0050
< 0.010
< 0 . 0050
< 0 .0050
< 0.0050
< 0. 010
< 0 .0050
< 0 .0050
< 0.0050
< 0.010
< 0.0050
< 0. 010
< 0.0050
< 0 .0050
< o. 0050
< o. 0050
< 0.0050
< 0,0050
< 0.0050
< 0.0050
< 0 .0050
< 0.0050
< 0.0050
< 0. 010
< 0.010
< 0.0050
Project Number: 61195.00-0003
Report Date Augunt 15, 2000
Page 1 of 1
Sample ID L00072001-22
Date Collected: 19-JUL-00 20:50
Date Received 20-JUL-OO
Qual RDL Units Analyst Data Time
0 .0050 mg/1 PAP 07/20/00 1238
0.0050 mg/1 PAP 07/20/00 1238
0.0050 mg/1 PAP 07/20/00 1238
0.0050 mg/1 PAP 07/20/00 1238
0.0050 mg/1 PAP 07/20/00 1238
0.0050 mg/1 PAP 07/20/00 1238
0.0050 mg/1 PAP 07/20/00 1238
0.010 mg/1 PAP 07/20/00 1238
0.010 mg/1 PAP 07/20/00 1238
0.0050 mg/1 PAP 07/20/00 1238
0.010 mg/1 PAP 07/20/00 123B
0 .0050 rng/1 PAP 07/20/00 123B
0.0050 rng/1 PAP 07/20/00 1238
0.0050 mg/1 PAP 07/20/00 1238
0.010 mg/1 PAP 07 /20/00 1238
o. 0050 mg/1 PAP 07/20/00 123B
0 .ooso mg/1 PAP 07/20/00 1238
0 .0050 mg/1 PAP 07/20/00 123B
0.010 mg/1 PAP 07/20/00 1238
0.0050 mg/1 PAP 07/20/00 1238
0. 010 mg/1 PAP 07/20/00 1238
0.0050 mg/1 PAP 07/20/00 1238
0.0050 mg/1 PAP 07 /20/00 1238
0.0050 mg/1 PAP 07/20/00 1238
0 .0050 mg/1 PAP 07/20/00 123B
0 . 0050 mg/1 PAP 07/20/00 1238
0.0050 mg/1 PAP 07/20/00 1238
0 . 0050 mg/1 PAP 07/20/00 1238
0.0050 mg/1 PAP 07/20/00 1238
0 ,ooso mg/1 PAP 07 /20/00 1238
o.ooso rng/1 PAP 07/20/00 1238
0.0050 mg/1 PAP 07/20/00 123B
0.010 mg/1 PAP 07/20/00 1238
0. 010 mg/1 PAP 07/20/00 1238
0.0050 mg/1 PAP 07/20/00 123B
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E-(f~rst Avenue I Greenwood, SC 29649 I [phone] I Filx (864) 229-71191
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D1\VIS
FLtwD LABORATORY ANALYSIS REPORT
client
r.·011tact
HNA HOLDINOS INC.
PO BOX B7
~HELBY, NC 28150
,lERRY MCMURRAY
Client IO: TRIP BLANK
Mc\t:rix
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1, 1,2, 2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1, J -DIC'!ILOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
GW/ChemW
Reault
< 0 .0050
< 0 .0050
< 0 .0050
< 0.0050
< 0.0050
< 0 .0050
< 0.0050
< 0. 010
< 0.010
< 0.0050
< 0.010
< 0 .0050
< 0.0050
< 0.0050
< 0.010
< 0.0050
< 0.0050
< 0.0050
< 0. 010
< 0.0050
< 0.010
< 0.0050
< 0.0050
< 0. 0050
< 0. 0050
< 0.0050
< 0.0050
< 0.0050
< 0 .0050
< 0 . 0050
< 0.0050
< 0 . 0050
< o. 010
< 0.010
' 0.0050
Project Number: 61195.00-0003
Report Date
Page 1 of l
Sample ID
Date Collected:
Date Received
Qual RDL
0.0050
0 . 0050
0 .0050
0.0050
0.0050
0 .0050
0. 0050
0 .010
o. 010
0.0050
0.010
0.0050
o. 0050
0.0050
0. 010
0.0050
0.0050
0 .0050
0. 010
0.0050
0.010
0.0050
0 .0050
0 . 0050
0. 0050
0.0050
0 .0050
0.0050
0 .0050
0 .0050
o. 0050
0.0050
0.010
0. 010
0.0050
Auguot 15, 2000
L00072001-23
18-JUL-OO 17; 05
20-JUL-00
Unit8 Analyst
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
Date Time
07/20/00 1214
07/20/00 1214
07/20/00 1214
07/20/00 1214
07/20/00 1214
01/20/00 1214
01/20/00 1214
07 /20/00 1214
07/20/00 1214
07/20/00 1214
07/20/00 1214
07/20/00 1214
07/20/00 1214
01/20/00 1214
07/20/00 1214
07/20/00 1214
07/20/00 1214
07/20/00 1214
01/20/00 1214
07/20/00 1214
07/20/00 1214
01/20/00 1214
07/20/00 1214
07/20/00 1214
07/20/00 1214
07/20/00 1214
07/20/00 1214
07/20/00 1214
07/20/00 1214
07/20/00 1214
07/20/00 1214
07/20/00 1214
07/20/00 1214
07/20/00 1214
07/20/00 1214
Davis & Floyd, Inc. I PO Drawer 428 \ Greenwood, SC 29648 I 8161, ~urst Avenue I Greenwood, SC 29649 ! [phone] I Fax [phone]
DAYIS
FLMD LABORATORY ANALYSIS REPORT
Surrogates % Recovery
Mea:rnreDate
L0007200l-Ol
L00072001-02
L00072001-03
L0007200l-04
L0007200l-OS
L0007200l-06
LOOO72DO1-O7
L00072001-08
L00072001-09
L00072001-10
L00072001-11
L00072001-12
L00072001-13
L00072001-14
L00072001-15
L000720D1-16
L00072001-17
L0007200l-18
L00072001-19
L0007200l-20
L00072001-21
L00072001-22
L00072001-23
LCS22629:1
MB22629:1
MS00072001-01:22629
MSD00072001-01:22629
LCS22640:l
MB22640:1
MSOD072001-19:22640
MSD00072D01-19:22640
20-JUL-00
20-JUL-00
20-JUL-OO
20-JUL-00
20-JUL-OO
20-JUL-OO
20-JUL-OO
20-JUL-OO
20-JUL-OO
20-JUL-00
20-JUL-OO
20-~1UL-00
20-JUL-OO
20-JUL-OO
20-JUL-00
20-JUL-OO
20-JUL-00
20-JUL-OO
21-JUL-00
21-JUL-OO
21-JUI,-OO
20-JUL-OO
20-JUL-OO
20-JUL-00
20-JUL-00
20-JUL-00
20-JUL-OO
21-JUL-DO
21-JUL-00
21-JUL-OO
21-JUL-OO
DCB
BFB
TOL
1,2-DICHLOROETHANE-D4
BROMOF l,UQROBENZENE
TOLUENF.:-DB
13 : 02
13 : 26
21: 04
14 :14
14 : 39
15 :03
15: 27
15; 52
16: 16
16: 40
17: 52
18: 16
18 : 40
19:04
19 : 20
19: 52
20 : 16
20: 40
09:18
10 :30
16:57
12 : 38
12: 14
21: 28
11: 42
17: 04
17:28
18:58
08 : 29
09: 42
10: 06
Report Date
Page 1 of 1
Matrix
Method
o·cE·-·· ":.":S'pf(.: ·· TOL
),\~AGi} \:{ci't-'~'1_:a_::>· ·g'Q\io_·;/::
111. 1 101.3 97. 6
113 .2 101. 0 95 .5
117 .B 100.7 94 ,6
110.B 100.2 96.5
112 .3 100.9 95.
112 .6 99.7 94 .1
113 ,3 99.1 95.l
111. 2 94.0 96.4
115. 5 101 . 2 93.7
117. 4 101. 6 93.4
116 .9 102.0 93 .7
117 .2 102.7 94 . 7
118.7 100.9 94. 0
119.2 100.7 93 . 3
118. 7 99.8 94 .7
120.4 101.3 93 . 0
114. 0 101.8 95 . 7
119.9 101.1 93 .4
107.3 99.4 95 .1
114. 9 102.4 ,S, 3
117. 7 102. 0 93 . 7
108.B 100.0 97 . 4
93.7 97.2 98.3
115.1 102.3 96 . 6
104.2 99.7 "· ' 125.6 102.0 92. 8
125.7 100. 9 93.3
120.5 103,0 94.4
106.7 101..3 95.9
l.15.4 102.4 94.8
120.6 103. 3 93.8
Auguot 14, 2000
GW/ChemW
SW846 8260
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Dav;s & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 EG9t"" Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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DAYIS
FLt1YD
Method Blanks
Blank
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-0ICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONB
BENZENE
BROMODICHLOROMETHANE
BROMOPORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CH LOR OM ETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
MB22629:1
LABORATORY ANALYSIS REPORT
Cone
< 0.0050
< 0 ,0050
< 0 . 0050
< 0.0050
< 0 .0050
< 0. 0050
< 0.0050
< 0.010
< 0.010
< 0.0050
< 0.010
< 0 . 0050
< 0.0050
< 0.0050
< 0. 010
< 0 ,0050
< 0. 0050
< 0 . 0050
< 0,010
< 0.0050
< 0.010
< 0.0050
< o.ooso
< 0.0050
< 0.0050
' 0.0050
< o.ooso
' o.ooso
< 0 . 0050
< 0. 0050
< o.ooso
< 0.0050
< 0. 010
< 0.010
< o.ooso
Report Date
Page 1 of
Matrix
Auguzt 14, 2000
GW/ChemW
WorkGroup: WG22629
Qual RDL Units Analyst Date
0.0050 mg/1 PAP 07/20/00
0 .0050 mg/1 PAP 07/20/00
o. 0050 mg/1 PAP 07/20/00
0.0050 mg/1 PAP 07 /20/00
0. 0050 mg/1 PAP 07 /20/00
0 . 0050 mg/1 PAP 07/20/00
0 .0050 mg/1 PAP 07/20/00
0.010 mg/1 PAP 07/20/00
0 .010 mg/1 PAP 07/20/00
0.0050 mg/1 PAP 07/20/00
0.010 mg/1 PAP 07 /20/00
0 .0050 mg/1 PAP 07/20/00
0.0050 mg/1 PAP 07 /20/00
0.0050 mg/1 PAP 07/20/00
0.010 .mg/1 PAP 07/20/00
0. 0050 mg/1 PAP 07 /20/00
0 ,0050 mg/1 PAP 07/20/00
0.0050 mg/1 PAP 07 /20/00
0.010 mg/1 PAP 07/20/00
0.0050 mg/1 PAP 07 /20/00
0. 010 mg/1 PAP 07 /20/00
0.0050 mg/1 PAP 07/20/00
0.0050 mg/1 PAP 07/20/00
0.0050 mg/1 PAP 07/20/00
0.0050 mg/1 PAP 07/20/00
0.0050 mg/1 PAP 07 /20/00
0 .0050 mg/1 PAP 07/20/00
0.0050 mg/1 PAP 07/20/00
0 . 0050 mg/1 PAP 07 /20/00
0.0050 mg/1 PAP 07/20/00
0.0050 mg/1 PAP 07/20/00
0.0050 mg/1 PAP 07/20/00
0.010 mg/1 PAP 07/20/00
0.010 mg/1 PAP 07/20/00
0.0050 mg/1 PAP 07/20/00
Time
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
1142
Davis & Floyd, Inc. [ PO Drawer 428 I Greenwood, SC 29648 I 816 Esrwrst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLt1YD
Method Blanks
Blank
Parameter
Volatile Organica
SWB46 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROBTHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HBXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENB
BROMODICHLOROMETHANB
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOR088NZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENB
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENB
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL}
MB22640: l
LABORATORY ANALYSIS REPORT
Cone
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
' 0.0050
' 0.0050
' o. 010
' 0 .010
' 0.0050
' 0.0.10
' 0.0050
' 0.0050
' 0.0050
< 0.0.10
< 0.0050
' 0.0050
' 0.0050
< 0.010
' 0.0050
' 0.010
< 0 . 0050
' 0 .0050
< 0.0050
' 0.0050
< 0.0050
' 0.0050
< 0.0050
' 0.0050
' 0 . 0050
< 0.0050
' 0.0050
' 0.010
' 0.010
' 0.0050
Report Date
Page 1 of
August 14, 2000
Matrix GW/ChemW
WorkGroup: WG22640
Qual RDL Unite Analyst Date
0 ,0050 mg/1 PAP 07/21/00
0.0050 rng/1 PAP 01/21/00
0 .0050 rng/1 PAP 07/21/00
0.0050 mg/1 PAP 07/21/00
0.0050 mg/1 PAP 07/21/00
0 .0050 mg/1 PAP 07/21/00
0 .0050 mg/1 PAP 07/21/00
0. 010 rng/1 PAP 07/21/00
0.010 rng/1 PAP 07 /21/00
0.0050 mg/1 PAP 07/21/00
0.010 mg /1 PAP 07/21/00
0.0050 rng/1 PAP 01/21/00
0.0050 mg/1 PAP 07/21/00
0.0050 mg/1 PAP 07/21/00
0.010 mg/1 PAP 07 /21/00
0.0050 rng/1 PAP 07/2.1/00
0.0050 mg/1 PAP 07/21/00
0.0050 mg/1 PAP 07/21/00
0.010 mg/1 PAP 07/21/00
0.0050 rng/1 PAP 07/21/00
0.010 rng/1 PAP 07/21/00
0.0050 mg/1 PAP 07/21/00
0.0050 mg/1 PAP 07 /21/00
0 . 0050 mg/1 PAP 07/21/00
0. 0050 mg/1 PAP 07/21/00
0.0050 mg/1 PAP 07/21/00
0.0050 rng/1 PAP 07/21/00
0 .0050 mg/1 PAP 07/21/00
0.0050 mg/1 PAP 01/21/00
0. 0050 mg/1 PAP 07/21/00
0.0050 mg/1 PAP 07/21/00
0.0050 mg/1 PAP 01/21/00
0 .010 rng/1 PAP 07/21/00
0. 010 mg/1 PAP 07/21/00
0.0050 mg/1 PAP 07/21/00
Time
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
0829
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DJvis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 Etters! Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
Parameter
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
·Parameter
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROBTHENB
Report Date
Page l of 1
Augu~t 14, 2000
Matrix GW/ChemW
MSD0072001-0l:22629
MSD00072001-0l:22629
WorkGroup: WG22629
Method SWB46 8260B
:·:_ij'pj_'k~·::\:· ·:.::F~~n\P_i:t:'' ··: "MS.:.
. ' A~d~l: . :?C6riif: ,•. ~~~-d
50.00
SO.OD
SO.OD
SO.DO
50.00
SO.OD
SO.DO
50. 00
50 .00
50 ,00
< 0.00500 53,03
< 0.00500 56.20
< 0.00500 52.65
< 0.00500 50.84
a.oases 57.31
Mso:
'~~c\.·
53.81 107.6
56.46 112.9
52.48 105.0
51.41 102.8
58.09 104.5
MS .. :··, -\R'i!c
106.1
112 .4
105. 3
101.7
102.9
1.46
0. 462
0.323
1 .11
1. 35
·:·t:Lifflt·t~
\REC
74-130
89-120
89-115
86-120
86-122
9
10
6
7
12
74-130
89-120
89-115
86-120
86-122
NOTE: MS/M~D % recoverieo are not evaluated if the sample concentration is greater than four timeo the opike added.
l,t/
Davis & Floyd, Inc. l PO Drawer 428 \ Greenwood, SC 29648 I 816 E.6rst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
Df\YIS
FLt1YD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
Parametc,r
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRIC!l!.OROETHENE
P_.ii.ran\eter
1,1-DICHLOROETHENE
BBNZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
Report Date
Page 1 of 1
August 14, 2000
MS00072001-19:22640
MSD00072001-19:22640
Matrix GW/ChemW
WorkGroup: WG22640
Method SWB46 8260B
. · ·-,:-:ip1i~·',:,,,,,-:-:-·,,:::-:'_jj'.-,;~i:~:/·:: -,,=:\NB\
·\td:'d:·:::•:._::d.:-.::'/;:.:. -.-.-.. -...... . ·.: -:·t:i"i~:{"t·~:>·'' -.
'"' :,' :\Egi)"g/:''" \;brif/'-•:·' · -. . -.-: ·\Ri:i.'Ct· .
SO.OD
50.00
so.co
50.00
50.00
so.co
so. 00
S0.00
so.co
S0.00
< 0.00500 53.58
< 0.00500 54.60
< 0.00500 53.19
< o.oosoo 52.50
< 0.00500 52.35
Sl. 34
53.90
52.02
50.75
51.38
102.7
107.8
104.0
101.5
102. 8
107.2
109.2
106. 4
105.0
104.7
4.27
1. 29
2.22
3.39
1. 87
\RBC
74-130
89-120
89-115
86-120
86-122
' 10
6
7
12
74-130
89-120
89-115
86-120
86-122
NOTE: M8/MSD \ recoverieo are not evaluated if the sample concentration ic greater than four t:imec the spike
0/ v✓o/-?-t)i)
(!_ 0 /J t
added.
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Davis & Floyd, Inc. j PO Drawer 428 \ Greenwood, SC 29648 I 816 E. Durst Avenue
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS
{>-~~~~ttie_ter
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
LCS22629:1
Report Date
Page 1 of 1
Matrix
Auguot 14, 2000
GW/Chemw
WorkGroup: WG22629
Method SW846 8260B
. s'p{k:e ':'>>:/LCs :_,-: -. .. . .· _:.·r.;cs ·=:>Liffii'til .
Acid~d' :;f(fi;Y:Jbid//:: ,:,·X\\kl~i/· =·-... :.)~~~-~:--.. ':
20. 00
20.00
20.00
20 00
20.00
20.76
21.78
21. 27
21.33
20.42
103. B
108.9
106. 4
106.7
102.1
74-125
90-119
89-116
87-120
B6-120
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] ! Fax [phone]
69
Df\YIS
FLtwD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS22640:l
-· :_·:'~-~·~ii~~~e;·
1, 1-DICHLOROETHENE 20 00
BENZENE 20 00
CHLOROBENZENB 20 00
TOLUENE 20 00
TRICHLOROETHENE 20 00
20.50
21.63
20.99
20.82
20. 29
Report Date
Page 1 of 1
: Augu□t 14, 2000
Matrix GW/ChemW
WorkGroup: WG22640
Method SW846 8260B
102. 5 74-125
108.2 90-119
105.0 89-116
104.1 87-120
101.5 86-120
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E7iurst Avenue I Greenwood, SC 29649 I (8641 229-4413 I Fax [phone]
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DAYIS
FLbYD LABORATORY ANALYSIS REPORT
Surrogates % Recovery
SampleNumber Mea::;ureDate
LOOD72001-04
L00072001-05
L00072001-06
L00072001-07
L00072001-0B
LCS22635:l
MB22635:1
MS0007200l-04:22635
MSD00072001-04:22~35
TBP
FBP
2, 4, 6-TRIBROMOPHENOL
2-FLUOROBIPHENYL
2FP 2-FLUOROPHENOL
NBZ
PHL
TPH
NITROBENZENE-05
PHENOL-OS
TERPHENYL-D14
27-JUL-OO
27-JUL-OO
27-JUL-OO
:?7-JUL-0O
27-JUL-OO
27-JUL-OO
27-JUL-OO
27-JUL-00
27-JUL-OO
17: 35
19: 26
2 0: 03
20: 40
21 ; 1 7
15 :46
15: 09
18: 12
:.a : 4 9
71 . 9 69.4
72.6 69,3
50.B 69.
77. 4 65 . 8
83 .6 1.06.1
79.7 65.J
72.3 62.0
64.7 68 . 4
75.B 67. 5
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue
71
Repo~t Date
Page 1 of 1
Augu~t 14, 2000
Matrix
Method
36. 4
35.4
27. 6
32.7
33 .8
36.8
37. 6
30 .5
34 . 3
GW/Chemw
SW846 8270
NEIZ. PHL·
26.7\09 · D-7O
73. 2 28.
72.5 29.0
7 2 . 1 25.4
69. 8 27.
50 . 2 28 . 3
68.2 29 .2
68.3 30.4
71. 1 26. 6
71. 6 27. 8
TPH
35-14
90.0
82. 6
88.3
84.2
72.9
89.2
84.8
87.0
87.7
I Greenwood, SC 29649 I 1864) 229-4413 I Fax [phone]
D1\VIS
FLOYD
Method Blanks
Parameter
Semivola.tile Organics
SWB46 B270C
1,2,4-TRICHLOROBENZENE
1, 2-DICHLOROBENZENE
1,3-0ICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2, 4, 6-TRICHLOROPJ-IENOL
2,4-DICHLOROPHENOL
2,4-DIMETHYLPHENOL
MB22635:1
2, 4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOR0PHEN0L
2-METHYL-4,6-DINITROPHENOL
2-METHYLNAPHTHALENE
2-METHYLPHEN0L
2-NITROANILINE
2-NITROPHENOL
3,3'-DICHLOROBENZIDINE
3-NITROANILINE
4-BROMOPHENYL PHENYL ETHER
4-CHLOR0-3 -MBTHYLPJ!ENOL
4-CHLOROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-METHYLPHENOL
4-NITROANILINE
4-NITROPHENOL
ACENAPHTHENE
ACBNAPHTHYLENE
ANTHRACENE
BENZO(A)ANTHRACENE
BENZO (A) PYRENE
BENZO(B)FLUORANTHENE
BENZO(G,H, l)PERYLENE
BENZO ( !<) FLUORANTHENE
BENZOIC ACID
BENZYL ALCOHOL
813(2-CHLOROETHOXY)METHANE
BI.S (2-CHLOROETIIYL) ETHER
BIS ( 2 -CHLOROIGOPROPYL) ETHER
LABORATORY ANALYSIS REPORT
Cone
< 0.010
< 0.010
< 0.010
< 0. 010
< 0,010
< 0 .010
< 0. 010
< 0.010
0 . 025
< 0 . 010
< 0 .010
< 0.010
< 0.010
< 0 .025
< 0.010
< 0. 010
< 0.010
< 0. 010
< 0. 010
< 0. 010
< 0.010
< 0.010
< 0.010
< 0 .010
' 0 .010
' 0.010
< 0. 025
< 0 .010
< 0. 010
' 0 . 010
< 0.010
' 0. 010
< 0 .010
< 0 .010
< 0. 010
< 0 .050
< 0 . 010
< 0.010
< 0 . 010
< 0 .010
Report Date
Page 1 of 2
Auguot 14, 2000
Matrix GW/ChemW
WorkGroup: WG22635
Qua.l RDL Unite Analyst Date
0 .010 mg/1 JRN 07/27/00
0.010 mg/1 JRN 07/27/oo
0 .010 mg/1 JRN 07/27/00
0.010 mg/1 JRN 07/27/00
0 .010 mg/1 · JRN 07/27/oo
0. 01.0 mg/1 ,TRN 07/27/00
0 .010 mg/1 JRN 07/27/00
0.010 mg/1 JRN 07/27/00
0 . 025 mg/1 JRN 07/27/00
0 . 010 mg/1 JRN 07/27/00
0.010 mg/1 JRN 07/27/oo
0.010 mg/1 JRN 07/27/oo
0.010 mg/1 JRN 07/27/00
0 .025 mg/1 JRN 07/27/00
0.010 mg/1 JRN 07/27/oo
o. 010 mg/1 JRN 07/27/oo
0 .010 mg/1 JRN 07/27/oo
0. 010 mg/1 JRN 07/27/00
0.010 mg/1 JRN 07/27/00
0 .010 mg/1 JRN 07/27/00
0 .010 mg/1 JRN 01/21/00
0.010 mg/1 JRN 07/27/00
0.010 mg/1 JRN 07/27/00
0 .010 mg/1 JRN 07/27/00
0 . 010 mg/l JRN 07/27/00
0 .010 mg/1 JRN 07 /21 /oo
0.025 mg/1 JRN 01/21/00
0. 010 mg/1 JRN 07/27/00
0 .010 mg/1 JRN 07/27/00
0 .010 mg/1 JRN 01/21/00
0.010 mg/1 JRN 01/21/00
0.010 mg/1 JRN 07/27/00
0. 010 mg/1 JRN 01/21/00
0.010 mg/1 JRN 07/27/oo
0. 010 mg/1 JRN 07/27/00
0 ,050 mg/1 JRN 07/27/00
0.010 mg/1 JRN 01/21/00
o. 010 mg/1 JRN 07/27/00
0 .010 mg/1 JRN 01/21/00
0.010 mg/1 JRN 07/21/00
Time
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
1509
l.509
1509
1509
1509
1509
1509
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DAYIS
FLtfYD
Method Blanks
Bl ctnk MB22635:l
Parameter
BIS(2-ETHYLHEXYL)PHTHALATE
BUTYL BENZYL PHTHALATE
CHRYSENE
DI-N-BUTYL PHTHALATE
DI-N-OCTYL PHTHALATE
DIBENZ(A,H)ANTHRACENE
DIBENZOFURAN
DIETHYL PHTHALATE
DIMETHYL PHTHALATE
FLUORANTHSNE
FLUORENE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEX.ACHLOROCYCLOPENTADIENE
HEXACHLOROETHANE
INOENO(l,2,3-CD)PYRENE
ISOPHORONE
N-NITROSODI-N-PROPYLAMINE
N-NITROSODIPHENYLA!1INE
NAPHTHALENE
NITROBENZENB
PEN"TACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRENE
SW846 8270C: DOWTHEP.1-1
1, 1' -BIPHENYL
BIPHBNYL ETHER
Prep Procedure Method
Analytical Prep Procedures:
BNA SEMIVOLATILE.S SWB46
DOWTHERM SW846
LABORATORY ANALYSIS REPORT
Report Date Augu~t 14, 2000
Page 2 of 2
Matrix GW/ChemW
WorkGroup: WG22635
Cone Qual RDL Unite Analyst Date Time
< 0 .010 0.010 mg/1 JRN 01/21/00 1509
< 0 .010 0 .010 mg/1 JRN 07/27/00 1509
< 0.0.10 0 .010 mg/1 JRN 07/27/00 1509
< 0.010 0.010 mg/1 JRN 07/27/00 1509
< 0 .010 0.010 mg/1 JRN 07/27/00 1509
< 0. 010 0.010 mg/1 JRN 07/27/00 1509
< o. 010 0.010 mg/1 JRN 07/27/00 1509
< 0 .010 0.010 mg/1 JRN 07/27/00 1509
< 0.010 0.010 mg/1 JRN 07/27/00 1509
0.010 0.010 mg/1 JRN 07/27/00 1509
< 0 .010 0.010 mg/1 JRN 07 /27 /00 1509
< 0 .010 0 . 010 mg/1 JRN 07/27/00 1509
< 0 .010 o. 010 mg/1 JRN 01 /21 /oo 1509
< 0. 010 0 .010 mg/1 JRN 07/27/00 1509
< 0 .010 0 .010 mg/1 JRN 07/27/00 1509
< 0 .010 0.010 mg/1 JRN 01 /27 /oo 1509
< 0 .010 0 .010 mg/1 JRN 07/27/00 1509
' 0. 010 0.010 mg/1 JRN 07 /27 /00 1509
< 0 .010 0 .010 mg/1 JRN 07/27/00 1509
< 0 .010 0 .010 mg/1 JRN 07/27/00 1509
< o. 010 0.010 mg/1 JRN 07/27/00 1509
< 0.025 0 .025 mg/1 JRN 07/27/00 1509
< o. 010 0 .010 mg/1 JRN 07/27/00 1509
< 0 .010 0. 010 mg/1 JRN 07/27/00 1509
< 0. 010 0.010 mg/1 JRN 07/27/00 1509
< 0 .010 0.010 mg/1 JRN 01 /27 /oo 1509
< 0. 010 0.010 mg/1 JRN 07/27/00 1509
Analyst Prep Data
3500B MCR 07/20/00 1145
3500B MCR 07/20/00 1145
Davis & Floyd, Inc. j PO Drawer 428 I Greenwood, SC 29648 I 816 Ef:rst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
Di\YIS
FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
11,'J/MSD
Parflmeter
1,1'-BIPHENYL
BIPHBNYL ETHER
1,2,4-TRICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4-DINITROTOLUENE
2-CHLOROPHENOL
4-CHLOR0-3-METHYLPHENOL
4-NITROPHENOL
ACENAPHTHENE
N-NITRO,SODI-N-PROl?YI,AMINE
PENTACHLOROPHENOL
PHENOL
PYRENE
·Parameter
1,1'-BlPHENYL
BIPHENYL ETHER
1,2,4-TRICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4-DINITROTOLUENE
2-CHLOROPHENOL
4-CHLOR0-3-METHYLPHENOL
4-NITROPHENOL
ACHNAPHTHENE
N-NITROSODI-N-PROPYLAMINE
PENTACHLOROPHENOL
PHENOL
PYRENB
MS00072001-04:22635
MSD00072001-04:22635
Report Date
Page 1 of 1
Matrix
Augu~t 14, 2000
GW/ChemW
WorkGroup: WG22635
Method SW846 8270C
,:·;;JPik~\ -~~¼£;:ft.· ..... ,.,.,_ MS':: _/::::)MSi::-
·,°'A:~·a;;tcr:·· ··:,··=·:\-'C6iiJ)r:·'·'·· ':':.:'./~i~~-~/<-_: ·.,. >\k-~c . /Liniit/
\REC
2B-128
26-123
32-92
29-92
37-115
35-97
44-102
4-71
40-104
39-106
11-126
4-70
43-112
50. 00
50.00
50.00
50.00
50. 00
75.00
75.00
75.00
SO.OD
50.00
75. 00
75.00
50.00
50. 00
50 . 00
so. 00
50. 00
so. 00
75.00
75. 00
75 .00
50.00
50.00
75.00
75. 00
50 . 00
' 0 .0100
' 0.0100
' 0.0100
' 0 .0100
' 0 . 0100
' 0.0100
' 0.0100
' 0 .0250
' 0. 0100
' 0.0100
' 0 .0250
' 0.0100
' 0. 0100
39 .39
34.84
29.44
30. 23
42.04
46.60
53.38
24. 28
JS. 95
36 .09
49. 09
20.68
42.80
39.14 78. 3
35.20 70.4
30.16 60.3
30.54 61 .1
39.36 78 . 7
41.90 55.
51.16 68 .2
19.09 2 5. 5
35. 07 70.1
)) .23 66.5
36. 91 49.
19. 17 25 .6
41.2B 82 . 6
7B.8 0. 637 20 28-128
69.7 1 . 03 1B 26-123
SB. 9 2 . 42 32 32-92
60 .5 1.02 35 29-92
B4 .1 6 .SB 25 37-115
62.1 10.6 31 35-97
71.2 4.25 21 44-102
32.4 23.9 27 4-71
71. ' 2.48 26 40-104
72 . 2 8.25 28 39-106
65. 5 28.3 2B 11-126
27 .6 7.58 2B 4-70
BS. 6 3.62 19 43-112
NOTE: M.S/MSD \ n~coverieo nre not eval\mted if the oample concentration io greater than four times the opike added.
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7
04-rst Avenue l Greenwood, SC 29649 I [phone] I Fax [phone] I
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DA,YIS
FLOYD LABORATORY ANALYSIS REPORT
Laborat01y Control Standards and Duplicates
LC.S
Parameter
1,2,4-TRICHLOROBENZENE
1, 4-DICHLOROBENZENE
2,4-DINITROTOLUENE
2-CHLOROPHEJ,JOL
4-CHL0R0-3-MBTHYLPHEN0L
4-NITROPHBNOL
ACENAPHTHENE
N-NITROSODI -N-i'ROPYLAMINE
PENTACHLOROPHENOL
PHENOL
PYRBNE
1,1.'-BIPHENYL
BIPHENYL ETHER
LCS22635:l
·s·p·~-~~\/
Added·
Les·:· :·:_::;:_tit/."'
50.00 27.08
50 00 26.82
50. 00 39.78
7 5. 00 42.47
75 00 49 .94
75. 00 26.39
50.00 33. 58
50. 00 31.14
75.00 48.92
75. 00 20 .41
50.00 41 .25
50.00 36 .30
50.00 32 .49
Report Date
Page 1 of 1
Augu::;t 14, 2000
Matrix GW/ChemW
WorkGroup; WG22635
Method SWB46 8270C
Les··. :i.iiffii'ti ·,:k~r/· \REC
54.2 31-96
SJ.6 31-93
79.6 39-114
56.6 34-101
66.6 44-102
)5.2 9-49
67.2 34-109
62.3 36-107
65.2 D-88
27.2 15-49
82.5 43-116
72.6 51.-102
65.0 43-108
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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DAYIS
FLOYD
Method Blanks
Blank
Parameter
aaa Chromatography
SW846 B0l.5
ETHYLENE GLYCOL
: MB22663:l
LABORATORY ANALYSIS REPORT
Repart Date
Page 1 of 1
Auguot 14, 2000
Matrix GW/ChemW
WorkGroup: WG22663
Cone Qual RDL Units Analyst Date Time
7.0 7.0 mg/1 JMT 07/26/0o 0233
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Davis & Floyd, Inc. I PO Dcawec 428 I Greenwood, SC 29648 I 816 E?°t'' Avenue I Greenwood, SC 29649 I 1864) 229-4413 I Fax [phone]
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DAYIS
FLffi'D
Method Blanks
Parameter
Gaa Chromatography
SW846 8015
ETHYLENE GLYCOL
MB22684:1
LABORATORY ANALYSIS REPORT
Cone
< 7.0
Report Date
Page 1 of 1
August 14, 2000
Matrix WW/STW/SFW
WorkGroup: WG22684
Qual RDL Onita AnalyBt Date Time
7.0 mg/1 JMT 07/31/0o 2036
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 I:. Durst Avenue I Greenwood, SC 29649 I [phone] \ Fax [phone]
77
DAYIS
FLMD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSO
Parameter
ETHYLENE GLYCOL
ETHYLENE GLYCOL
MS00072U01-02:22663
MSD00072001-02:22663
Report Date
Page 1 of 1
Augu~t 14, 2000
Matrix GW/CheroW
WorkGroup: WG22663
Method SW846 8015
),~P\ff)J/: '="-:::::-~~¥I{L~=::::,:-= ::}::"MS:::-:·-·.=-··--.-.·❖-.:= =-:\IS::/.:· ····-·.-.. --£I~[~¥":\·:··
Added... ·::g}Jf·· ··)'d;ik/ "°":\~~~--:·= ··.,.-\R·Ec·
50.00 < 7.00 50 .39 100.8 73-116
·.·.·::M's·o< · .. Limi't':J . <JR·~-~ \f_"~i5° \REC
50.00 53.95 107.9 20 73-116
NOTE: MS/MDD \ recoverieo are not evaluated if the oample concentration io greater than four timeo the opike added.
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Dav;, & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 Els''' Avenue I Greenwood, SC 29649 I 18641 229-4413 I Fax {864) 229-7119 I
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Df\YIS
FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
· .. ::'.Parameter
BTHYLENB GLYCOL
·. :: Piirameter
ETHYLENE GLYCOL
M.S/MSD
Report Date
Page 1 of
Auguot 14, 2000
Matrix WW/STW/SFW
MS00072001-03:22684
MSD00072001-03:22684
WorkGroup: WG22684
Method
.. SPik~ .. ·_:.:-sacip_1~\:,: :. Ms
-·Aaded :<:)::C:6'rib/-:··· cone
500.0 802.4 1280.
500.0 1293. 98.2
SW846 8015
MS
\RBC
95.5
\REC
68-115
L'iniit's'
·'tRPo i\-~s_(:'=./:
20 68-115
NOTE: MS/MSD \ recoverie::; are not evaluated if the oample concentration is greater than four times the opike added.
Davis & rloyd, Inc. j PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (B64) 229-4413 I Fax {864) 229-7119
79
DAYIS
FLt1YD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
_.Parameter
ETHYLENE GLYCOL
LCS22663:l
Report Date
Page l of 1
Augu□t. 14, 2000
Matrix GW/chemW
WorkGroup: WG22663
Method SWB46 8015
spike<,'·. ··:,,:·::'LC:'S· · Les < .Li~i t:n
. Ada~a··_:c::.:"::'<' :-.:~iric:,i• }}?·i:::\;~i~., _.-.: \REC
50.00 45. 44 90.9 64-117
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue \ Greenwood, SC 29649 I [phone] I Fax [phone]
80
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DAYIS
FLtrYD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
Parameter
ETHYLENE GLYCOL
LC.S LCS22684:1
sl)ik~\ .. : //Le's··
Added , i/tb·;;~·-.,_:·
50.00 51.08
Report Date
Page 1 of l.
Auguot 14, 2000
Matrix WW/STW/SFW
WorkGroup: WG226B4
Method SWB46 8015
,LCS ··
\-REC:
102.2
.: L:{fflits
\-REC'.
64-117
Davis & Floyd, lnc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
81
DAYIS
FLOYD
Method Blanks
Parameter
Wet Chemistry
SW846 !1060
Blank
ORGANIC CARBON, TOTAL
MB22702:1
LABORATORY ANALYSIS REPORT -
Cone
< 1.0
Report Date
Page 1 of 1
Augu::;t 14, 2000
Matrix GW/ChemW
WorkGroup: WG22702
Qual RDL Units Analyst Date Time
1. 0 mg/1 TRB 07/27/00 1620
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Davis & Floyd, Inc. I PO D,awe, 428 I G,eenwood, SC 29648 I 816 Es°f"' Avenue I G,eenwood, SC 29649 I [phone] I Fax [phone]
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DAYIS
FLtwD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MG/MSD
Parameter
ORGANIC CARBON, TOTAL
:~arameter
ORGANIC CARBON, TOTA[,
MS00072003-0l:22702
MSD00072003-0l:22702
·::1:1::{-'?:
20.00
20.00
Report Date
Page 1 of 1
Matrix
August 14, 2000
GW/ChemW
WorkGroup: WG22702
Method SW846 9060
.::/,s~~Pi'~ · ··:.:-:-Ms· : .. :Ms : ··\~6ri~':\('"' . -·::};;~:6:_:,,:•:· ·:-' _:·._:::_:·,i~2·
9.83 30.70 104.4
31. 00 109.9
. -.iXmi t·d· · .-,~-~t>'"
77-121
17 77-121
NOTE: MS/MSD \-recoverieo are not evaluated if the sample concentration i::i greater than four timeo the opike added.
Davis & Floyd, Inc. j PO Drawer 428 j Greenwood, SC 29648 I 816 E-f1rst Avenue I Greenwood, SC 29649 \ {864) 229-4413 I Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
: LCS22702:1
\\;~Lmet~~
ORGANIC CARBON, TOTAL 10.00 10.70
Report Date
Page 1 of 1
Matrix
Augunt 14, 2000
GW/ChemW
WorkGroup: WG22702
Method SW846 9060
107,0 90-110
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Dav;s & Floyd, Inc. I PO D,awec 428 I G,eenwood, SC 29648 I 816 EaDJ"sl Avenue I G,cenwood, SC 29649 I [phone] I Fax [phone]
- --- -- - -----Chain of Custody Record
Client 816 E. Durst Avenue, Greenwood. SC 29649 [phone] Fax: [phone]
Laboratory Certifcalion Numbers: SC-24110, NC-25, TN-2923, VA-77 C.NA Holdings
Shelbv,NC
Contact
Project I Site Location
61195.00/0003
Plant Site
Copy To Reporting Requirements: { } Standard ~ Data Package (Specify Level)
co
c..n
Johnnv Ledford
CoJlecied By
NOTICE:
Samnle Descriotion
r--r e. :r:.
,:./ ,✓_ 7 7
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Samo!e Collection
Date Time
-,. ,,;_.,, o 4 l/J
Time
()"? 'JO
Time
llof z_...
Reliquished By
Received By
-~ 8. E 8
Time
),(v ,B ,I'/. -/vA JL
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x .,--LJ ?
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Date
Date
Required Parameters, Containers and Preservatives
E " • Ji-~ g C)
~ 0 • 0 t) ~ 0 e i; w
B A A
I l,
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1)
t
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Time "'eliquished By Date
Time Received in LabOl"ato,y By Date
ti 5/J /II . DJ /1 ,/, 5 T.lo.oo
Matrix Type DefUlitions 1 -Drinking Water 2 -Clean Water 5. Groundwater 7 -SoiVSediment 8 -Liquid Sludge 9 -Oil 12 -Air
PreseNalive Definitions A -None B -H2S04 C • HCI D -HNOJ E • NaOH F -Filtered G -Other
Time
Time
OJBO
--Page_/_ot_2_
ice use univ
Purchase Order
State Quote
..J
Fraction HOT t;omments
QI
0.3
06
Of.,
07
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Quick~
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If Y, specify:
r days
'"""
Airbill Number
Cooler ID (if available): _,,_./'--~-
On Ice: QNo Temp(C) /J.
Custodv Seal: Intact / Brok.en~
Davis & Flora, me.
FL02 _01 (0Z/99)
0:,
C,
D~IS"'""""' ?r.:'. wumre
FL YD 1mr..-.i • """""15'.nira
Client
C.NA Holdings
Shelbv.NC
Contad
Project I Sile Location
61195.00/0003
Plant Site
Rep"'!P ,<,1 A '
Johnnv Ledford J A",1..,v h'Jf, J]_' ~ A 1
Chain of Custody Record Page__2_ar.2_
816 E. Durst Avenue, Greenwood, SC 29649 [phone] Fax: [phone] vulCe use
Laboratory Certifcation Numbers: SC-24110, NC-25, TN -2923, VA -n
Reporting Requirements: { ] Standard .9<:[_ uala Package (Specify Level)
Copy To
Jc J H.6J., r-I~ ii
Purchase Order
Collected By / _ /. / t, t, Required Parameters, Containers and Preservatives State Quote
t--------,,==~:::--'_J, __ n __ /'-1_-,<'_Y¼. __ ~ __ a_._~ •--,----+-r--r--r---+~i-t-'~~"-t-~!~t-'~~~t-'--t---t-'--+--+---t--+---t--+"~o-,o~~-n-jc-;---j/Specia
/

Ins/ructions
NOTICE:
I? :;;
C
'a 0 • ~ "C ~ : s Cl.
Samole Collection E -~ ~ c:2~
• l D E 0 e
" " Samele Descrintion Date Time Time Tyµe
,;;-~ -3 f-7-/f,,r, lf'l< )(
,::' ,:;--It{.? , i'. '1 ., y
C, /.:, -✓-/ /9 "% .;-y
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Total C
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Date
E 0 " !'. ~ , 5 0 • 0 C u • " ! 0
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Time Re/iquished By Date Time
C ~,,; ~ . .,,
0 • C S
t-... ~_g
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• u c::, i5 ~
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Fraction HOT ommems
16
11
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Q~ick ~ Ship~ cuENT
U" rreceived By Date Time Received By Date Time Date Time
7.UlCO 0730
v r.c='-;;!-5''==-~'~"="' --; If Y, specify: Airbill Number
/ days
1......,.,.,,.ents Cooler ID (if available): /
On Ice: @ No Temp(C) t.J..
Custody Seal: Intact t Broke,n--;Q.,
Matrix Type Definitions 1 -Drinking Water 2 • Clean Water 5 -Groundwater 7 • SoiUSediment 8 -Liquid Sludge 9 ~ Oil 12 • Air
Davis & Floyd, Inc.
Preservative Definitions A -None B -H2S04 C -HCI O -HN03 E • NaOH F • Filtered G • Other
FL02 _ 01 (02199) ----------

-
----
I
1D1'}118 CHGIH((RS ARCHITCCTS
. FLfil'D rl.At-lNCRs sc1cHnsrs
FIELD DAT A LOG
I CHARLESTON • G,RCENWOOD • COLUMBIA
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
. Well No· TTCT. . .
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cnent: C!/d-/h!,/,nq.S. z:,,, "-Source(s) of Well ID Ma,, . L ID Lob '~no)
✓ , I
Site Name: 5"be/by, ,1-JC Job Ho.:/ 110'5.o ' Well Completion: Protective Casing @/no) ush (yes@
Dale: z·-J'.l: ZOoc, LWR submilled by: ,-M-nush-lJount Cover Seal Intact (yes@ eking Cap (yes@)
'
Sampling Personnel: JLM L,/4/~ Locked al Arrival (yes/n 0 Depa re (yes/no)
-2
Site Personnel: Well Casing eight b I) below) ground: " ep
Regulatory Personnel: ~ Casing Type (PVC) I 1/ ~!her)
Weather Condillons: C ,< O,JiJ 'l Temp.: @ 1~ Oedicate~o B er (yes/no) Type
I
Well Oiameier. z.,,., In.~ Protective Post/ lmenl (yes/no) Concrete Pad @/no)
(A) Top of Well £1evation: G /£. .4-~ Well Integrity alisfactory (yes/no) If no, explain below. 4 msl (yes/no)
(B) Depth to Immiscible Layer. -n/ Well Yiel ( low / moderate / high )
(C) Immiscible Loyer [fevation: (A)-(B)-' c... msl (yes/no) 7·
(D) Depth to Groundwater. ft. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(D)= msl (yes/no} DIA. OF PIPE (in.) VOLUME IN GAL/R.
1.0 0.041
(F} Total Well Depth = ft. 2.0 0.163
3.0 0.367 ·
(G} length of Waler Column: (F)-(D)= fl. 4.0 0.653
. ,v 5.0 .. 1.020
Casing Volume = (G) x Volume in gal./rt.-gals. 6.0 t.470 -
Method of Well Evacuation p,.,_tzl p. Start Time: -TO CONVERT GAi/FT TO UTERS/FT, MULTIPLY ABOVE nGURES BY
Method of Sample 'Collection ?u. w: l) Time: oil £.( ?
3.8 UTERS/GALLON.
I '
Chain-of-Cu,tody Form Storied ®/no)
FIELD ANALYSES
tst Volume 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged (gallons)
Time (mmtary) ,:,,;1J
pH (S.U.) r~
Sp. Cond. (umhos/ cm) IC\,.., ..........
Water Temp. ("c) > -
Odor (subjective)•
Turbidity (subjective)"
• (!}None (2)Slighl (3)Moderole (4)Slronge
" (l}cleor (2)Slighlly Turl>id (3)Moderalety Turt,id (4)Very Turl>id (S)Exlremely Turl>id
Comments/Observolions/Recommendalions: ------------------------------
,,., """"" z,ii?&h (SICMAIIA)
o , 7-l'1ct20
01,: r rorm4B (3/94)
87
[HGIH[[RS ARCHITtCTS FIELD DATA LOG D/\}/1S
FL6YD PLANNERS SCIEHHS(S
CHARLESTON • C_REEHWOOD • COLUMBIA
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
Well ..
Client: r' J/.d_. J/,z/i!/05, £>1. <!. Source(s) of Well ID M.a,, ID Lobel es no)
./ 7 I
Sile Hame:Sbe / b T, /JC Job Ho.: / I I C7 5. 0"1'5JO:> Well Completion: Proteclive Cosing @/no) sh (yes@)
Dole: Z -l 1 ZOoc, LWR submitted by: ~ nush-Mounl Cover Seal Intact (yes,(§) L ing Cop (yes~
Sampling Personnel: JLt:J Lu/~ Locked al Arrival (yes/no Oeporl e (yes/no)
7
. , f/4, elow) ground:
Sile Personnel: -Well Cosing fheighl obo ~
I,
Regulatory Personnel: -Cosing Type (PVC) ( J, !her)
Temo.,8i7 j ' Weather Conditions: (2nQ.l)v Dedicate~ or I a er (yes/no) Type
I
Well Oiameler: z.~ In. Protective Post/ tmenl (yes/no) Concrete Pod @/no)
(A) Top of Well Elevation: , r / Lf. mst (yes/no) Well lnlegri otisfaclory (yes/no) If no, explain below.
(B) Depth lo Immiscible Loyer. /_ I. Well Yi ( low / moderate / high )
(C) Immiscible Loyer Elevation: (A)-(B)= -msl (yes/no)
(0) Depth to Groundwater. ft. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(0)= msl (yes/no)
DIA. OF PIPE (in.) VOLUME IN GAL/Ft.
1.0 0.041
(F) Total Well Oeplh = ft. 2.0 0.163
3.0 0.367
{G) Length of Water Column: (F)-(0)= fl. 4.0 0.653
\. I /
5.0 .. 1.020
Cosing Volume = (G) x Volume in gol./ft.= Qols. 6.0 1.470
-
Method of Well Evacuation P(.,,...ia:i f2 Start Time: TO CONVERT GAL/FT TO UTERS/FT, MULTIPLY ABOVE FIGURES BY
Method of Sample tolleclion ?u.ruD Time:Of I'. I
3.8 UTERS/GALLON.
I
Chain-of-Custody rorm Started ®/no)
Gr-a. b FIELD ANALYSES
1st rf'0la1M" 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged (gallon~)
Time (mmtary)
pH {S.U.) .;::r-, L
Sp. Cond. (umhos/ cm) .2 ..,,,... -
Waler Temp. (•c) z.. 7
Odor (subjective)•
Turbidity (subjective)"
• (1)None (2)Slighl (3)Moderole (4)Slronge
" (1 )Clear (2)Slighlly Turbid (3)Moderolety Turbid ( 4)Very Turbid (5)£xlremely Turbid
fl
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Comments/Observalions/Recommendalions: ------------------------------1
O& f form48 (3/94)
88
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1D.t\l'IS ENGINEERS ARCHITt:CTS FIELD DAT A LOG
-FL{j\7D PlANH(RS SCl(HHSfS
I CHARLESTON • G_REENWOOD • COLUMBIA
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
Well No • f> Ew -l -..
Clienl: f" JJ.,I-J/,,z.4/t_ttq.,r,_, Z:,t_~ Source(s) of Well ID Mt1n ID label (§y'no)
.,/
I
Sile Home:Sb,., / by, 1JC Job Ho.:/ 1105.o
, Protective Cosing @/no) Well Completion: flush {yes@
Dote: z·-,q-ZOe:>o LWR submilfed by: AW nush-Mount Cover Seal Intact (yes.<§} Locking Cop {yes@)
Sampling Personnel: JLtJ 7 u,/0,/ Locked al Arrival (ye~ Departure (yes§}
Sile Personnel; -Well Cosing (€eight ob~/deplh below) ground: I --. -> fl,
Regulatory Personnel: --Cosing Type (PVC) ~(Other)
Weolher Condition,('/. -vd:<;} $(, I Dedicate~ or Bailer (yes/no) Type -Temp.:%> '>
Well Diomeier: t1f, 0 In. Proleclive Posl/Abulmenl y;;/no) Concrele Pod @/no)
(A) Top of Well Elevation: f'~,?, g~· msl (yes/no) Well Integrity Solistoctory~o) It no, explain below.
(B) Depth lo Immiscible Loyer. -fl. Well Yield ( low / moderate / ~ )
(C) Immiscible Layer Elevation: (A)-(B)= -msl (yes/ no)
(D) Depth lo Groundwoter: <It .. 08 fl. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(D)= ]'"z, o, Z Z msl (yes/no)
DIA. or PIPE (in.) VOLUME IH GM../Ft.
1.0 0.D41
(F) T olol Well Depth = 'i'{ Ia ft. 2.0 0.163
3.0 0.367
(G) Length of Waler Column: (f)-(D)= "1 2-: ;! 2-ft. 4.0 0.653
5.0 .. 1.020
Cosing Volume = (G) x Volume in gol./tt.= ,,~--,~ gals. 6.0 1.470 -
Method of Well Evacuation p,.,_ /:ZJ f,. Start Time;(<?.? i, TO CONVERT GAi/FT TO UTERS/FT. MULTIPLY ABOVE RGURES BY
Method of Sample "Collection ?t.<. m /) Time:/,zf"Z-
3.8 UTERS/GALLOH.
I
Chain-of-Custody form Started @/no)
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3 'Z"] 75 J'] FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged (gallons) t: ,,-;5"' 13 3-o ~4'9, .J-
Time (military) I -, -' ,J M '7 -/~ ,._-,
pH (S.U.) f, z .,. -f <'-: ,/
Sp. Cond. (umhos/cm) f7 4,,: ~,b
Waler Temp. {"C) .2 I ;:, ,., :,_,:,
Odor (subjective)• -, I I
Turbidity (subjective)"" , ' I
• (1)Hone (2)Slighl (3)Moderole (4)Slronge
" (!}Clear (2)Slighlly Turbid (3)Moderolely Turbid (4)Very Turbid (5)Exlremely Turbid
Comments/Observations/Recommendations: o ✓• I_ .i
(~II.It()
, 2 -1 e-1211
I
Ok r rorm48 (3/94)
89
I
CNCIHCERS ARCH1f£CTS Df\YIS
FLGYD PLANNERS SCIEHIISIS
FIELD DAT A LOG I
FOR GROUNDWATER SAMPLE COLLECTION/
CHARLESTON • G/lEENWOOO • COLUMBIA -..
Client: CA/tf-l/4,lql,qs;,, hn <!-Source(s) of Well ID M,,,, ID Lobel (§!no)
I
Sile Name:Sbelby, ,A/C Job No.:/ 1!<75.o
, Protecltve Cosing @/no) Well Complelion: Flush (yes@
GROUNDWATER ELEVATION MEASUREMENTS _ :-;.
· Well No • fie p-> a I
Date: Z ·L f_· ZOoc, LWR submitted by: /1/4_ nush-Mount Cover Seal lntacl (yes@ locking Cap (yes@)
Sampling Personnel: JLlj 7 /4:YJr,/ locked at Arrival~no) Oeparlur@/no)
Sile Personnel: -Well Casing ~ighl ab~/deplh below) ground: Z-o (I,
Regulatory Personnel: -Casing Type (PVC) e (Other) -
Weather Condilion ✓.--'/4<>""'--'o/-::: T emp.:&'65' Dedicate~ or Bailer (yes/no) Type -
Well Diameter: z. ~ In. Protective Post/ Abutment (yes/ no) Concrete Pad @/no)
(A) Top ot Well Elevation: zt~4g mst (yes/no) Well Integrity Salistaclory (yes/no) If no, «plain below.
(B} Depth to Immiscible layer: -fl. Well Yield ( low / moderate / high )
(C) Immiscible Loyer Elevation: (A)-(B)= -msl (yes/no)
(0) Depth to Groundwater. °3 6..-7 C. ft. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(D)-1£7 . 7 ,Z, msl (yes/no)
DIA. or PIPE (in.) VOLUME IH GAL/ft.
1.0 0.041
(f) Total Well Depth = '2.-,g_ocJ ft. 2.0 0.163
? !._-z tf_
3.0 0.367
(G) Length of Woler Column: (f)-(0)= ft. 4.0 0.653
5.0 .. 1.020 --Casing Volume = (G) x Volume in gaL/ft.= ~. _;, gals. 6.0 1.470 -
Method of Well Evacuation Pv...""' p Start Time: / J ~ (2 TO CONVERT GAL/FT TO UTERS/FT, MULTIPLY ABOVE FlGURES BY
Method of Sample tollection PL<-a1 /'\ Time:/t/o 7 3.8 UTERS/GALLON.
I
Chain-of-Custody form Started @/no)
FIELD ANALYSES
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1st Volume 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged {gallons) ~.,. .,-7_J /c>. ~-
Time (military) /:,.do / ,l .,-._ -

;

<,' ~ ~----
pH (S-U.) 6 _---;:; ,_ ? / -z_
I
Sp. Cond. (umhos/ cm} .., /' J.,_ '7Z. 7 'l.-I Waler Temp. {°C} , .. 18" I$'
Odor (subjective}• I / I
Turbidity (subjective)" ' J I
• (t}Hone (2}Slighl (3}Moderole (4}Stronge I
" (t)Cleor {2}Slighlly Turbid (3)Moderotely Turbid (4)Very Turbid (S)Exlremely Turbid I
Comments/Observolions/Recommendalions: _________ _____:, ____________________ , I
----~-------,/-+------,"t-.1
I
o& r rorm48 (3/94)
90 I
I
ID l\}11 s £HG1H((RS ARCHIITCTS FLmro Pl.ANHCRS SCl[HHStS
FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS I CHARLESTON • G_REENWOOD • COLUMBIA , Well No • C. c '3 J .. -
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er.en!: f'7 Jid_. J/4.~d o S, -:Z:,,, e. Source(s) of Well ID Ma.a ID Label @'no)
/7 I
Site Name:Sbelby, ,A.IC Job No.:/ 11<?5.o~' Well Completion: Protective Cosing @/no) Rush (yes@
Dole: Z • £ ( -Z Ooo LWR submilled by: Al tJ.. nush-ijount Cover Seal Intact (yes.{§) Locking Cop (yes~
Sampling Personnel: JLM l lj,//"Jt/ Locked al Arrival ~/no) Ocporture~/no)
Site Personnel: -Well Cosing ~ighl ob<0/deplh below) ground: z.. 2 !I,
Regulatory Pmonnel: -Cosing Type (PvC(9 (Other) -
Weather Conditions: t'/4« .. ,y Temp.J"tJ's Dedicate~ or Boiler (yes/no) Type -
Well Diameter. ? . ,,-, In. Proleclive Posl/Abulmenl (yes/a} Concrete Pod @/no)
(A) Top of Well [levolion: if' I 2. '-i? msl (yes/no) Well Integrity Solis(oclory~no) If no, explain below.
(8) Oeplh to Immiscible Layer. -ft. Well Yield ( low / moderate / ~ )
(C) Immiscible Layer Devotion: (A)-(8)= -ms! (yes/ no)
(0) Depth to Groundwater. z. tJ_. 1L/ ft. WELL VOLUME DATA
(E) Groundwater [tevation: (A)-(0)= ZRB-~t msl (yes/no)
DIA. or PIPE (in.) VOLUME IN GAL/ft.
1.0 0.041
(f) Total Well Depth = y J.00 ft. 2.0 0.163
3.0 0.367
(G) Length of Water Column: (f)-(D)= &'.5, ft. 4.0 0.653
5.0 .. 1.020
Casing Volume = (G) x Volume in gal./ft.-l, f gals. 6.0 1.470 ..
Method of Well [vocuolion PL,..!:!'.) f!. Start Time: o"[OO TO CONVERT GAL/FT TO UTERS/FT, MULTIPLY ABOV[ RGURES BY
Method of Sample Collection ?(-<,m/) Time: '2 ,; / </ 3.8 UTERS/GALLON.
I
Chain-of-Custody form Storied @/no)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged (gallon~) I ,q . ~-" A_<'
Time (military) 04 O!,-~ d , ,.,, ;1 (J/ 2...
pH (S.U.) ... 4' «;---9 .t.o
Sp. Cond. (umhos/cm) /(:}/ ;,4,J 7"-.>-
Water Temp. (•c) , ,tf , <? /'Ii'
Odor (subjective)' I I I
Turbidity (subjective)" I I I
• (l)None (2)Slight (3)Moderale (4)Stronge
" (1 )Cteor (2)Slighlly Turbid {3)Moderolely Turbid (4)Very Turbid (S)Exlremely Turbid
Comments/Observo1ions/Recommendalions: ------------------------------
D& r form48 (3/94)
91
[HGIHCERS ARCHITCCTS FIELD DAT A LOG
PLANNCRS SCICHIIStS
DJUIIS
FLffi:D
CHARLESTON • C_REENWOOO • COLUMBIA
Cfienl: (j(/1. J&J/u'jS,, &t"-·
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
-
Source(s) of Well to Man
Well .. -.
I
I I) 4-p
No·PEw c.,, I
to Label @,'no)
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Site Name:Sb,./61, tJC Job No.:,( lic?S.o/4 1· Well Complelion: Prolective Casing @/no) Flush (yes@
Dale: Z • /'J.· ZOOo LWR submilted by: 4t.l. flush-lJounl Cover Seal lntocl (yes@ Locking Cop (yes~
Sampling Pen:onnel: JLn 7 lj,/,Q,/ Locked of Arrival (yes/iii,} Deporlure (yes,@,)
Sile Personnel: -Well Casing (!5e,ghl ab~/dcplh below) ground: ;>. ,:;:,'l a.
Regulatory Personnel: ~ Casing Type (PVC)@ (Other) -
Weather Conditions: C/4«41 Temp.:'72> •~ Dedicate~ or Bailer (yes/no) Type -
>
Well Diameter: e, Q In. Proleclive Posl/Abulmenl (yes/no) Concrete Pad @/no)
(A) Top of Well Elevation: 6Lj ~-ZY msl (yes/no) Well Integrity Satisfactory (yes0) If no, explain below.
(8) Depth to Immiscible Layer: -ft. Well Yield ( low / moderate / ~ )
(C) Immiscible Layer Elevation: (A)-(8)= -msl (yes/ no)
(D) Depth to Groundwater: Y7.tf6 ft. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(D)= ? l I ,-5' 7 msl (yes/no)
DIA. or PIP[ (in.) VOLUME IN GAL/Ft.
1.0 0.041
(F) Total Well Depfh = f5",,90 ft. 2.0 0.163
3.0 0.367
(G) Length of Waler Column: (F)-(D)= :>~7. ,2'. Z, fl. 4.0 0.653
~ '-/, ·3
5.0 .. 1.020
Casing Volume = (G) x Volume in gat./fl.= gals. 6.0 1.470 .
Method of ·Well Evacuation p'-'-IZ! f2 Starl lime:/b' z:<t TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOVE FlGUR[S BY
Method of Sample Collection y,.,_l:21 A lime: 11 -z p 3.8 LITERS/GALLON.
I
Chain-of-Custody farm Storied (fi)/no)
JCJ)l'87 FIELD ANALYSES ltf. '~~,o
1st Volume 2nd Volume 3rd Volume 6th Volume
Volume Purged (gallons) .f"-1 /,f £' ... .;;,.s.3<1 -
lime (military) ) /6 ~-, I I .> 11 Z-7 ,, 7-.,
pH (S.U.) ,_ I C. _. &, I / ,
Sp. Cond. (umhas/cm) ..-"' ....... <J .-Cl
Waler Temp. {°CJ z-z. i! z._ z z._. , :z
Odor (subjective)• I I I I
T urbidily (subjective)" J I L J
'
• (1)Nane (2}Slighl (3)Moderole (4)Slronge
" (!)Clear (2)Slighlly Turbid (3)Moderolely Turbid (4)Very Turbid (5)Exlremely Turbid
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Comments/Observotions/Recommendolions: _ _j_/{:i...1,l!?~/.,b...!a,e:..<.<:.1.k;..__ _____________________ ,
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ID 1'}/1 S ENCIH(ERS ARCHITECTS FLmro PUHN(RS SCICHHSfS
FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS I CHARU:STON • G,REEHWOOO • COLUMBIA . Well No · PIEw-c-J .. -
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Client: CA/J-f/4//t115s,, M <! Source{s) of Well IO Ma.a IO Lobel @'no)
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Sile Hame:Sh,.. /by, ,Al C Job Ho.: / I !OS. o ·' Well Completion: Protective Cosing @/no) nush {yes~
Oale: Z • t_q_-zooo LWR submilled by: IV ,1_ nush-tJounl Cover Seal lnloct (yes@ locking Cop (yes@}
Sampling Personnel: JL!j 7 lw.rv Locked al Arrival {yes~ Oepar1ure {yes0J
Sile Personnel: -Well Cosing ~ighl ab<ii}/deplh below) ground: Z-2'
Regulatory Personnel: Casing Type {PVC) ~ {Olher) -
Weather Conditions: {&,,. ,f'j Temp.::zbs Dedicate~ or Bailer (yes/no) Type -
Well Diameter: ($: 0 In. Prolec!ive Post/Abulmenl ([,!')/no) Concrete Pad @/no)
{A) Top of Well [levalion: ~ ~i. l '--t msl (yes/no) Well Integrity Salisfoctory {yes/@) If no, explain below.
(B) Depth to Immiscible Layer: -ft. Well Yield { low / moderate / ~ )
(C) Immiscible Loyer aevalion: (A)-(B)= -ms! {yes/ no)
{O) Depth to Groundwater: 34 7:,~ ft. WELL VOLUME OATA
(£) Groundwater Elevation: {A)-(0)= '5 I ? • ..J f ms! (yes/no)
OIA. Of PIPE (in.) VOLUME IH GAL/fl.
1.0 0.041
(f) Total Well Depth = C/J. Ji> ft. 2_0 0.163
':> -{? Y) 3.0 0.367
(G) Length of Water Column: {f)-(0)= ft. 4.0 0.653
5.0 --1.020
Casing Volume = (G) x Volume in gal./ft.= %~ gals. 6.0 1.470
Star1 Time: It' ,;d: Melhod of Well Evacuation 'R,._1:2:l P-TO CONVERT GAl/fT TO UTERS/fT, MULTIPLY ABOVE nGURES BY
Method of Sample ·eonection ?"-at/'> Time: J z,::, p
3.8 LITERS/GALLON.
I
Chain-of-Custody r orm Star1ed @/no)
2 9z "77 7
FIELD ANALYSES
Volume Purged (gallons)
Time (mmlary)
pH {S.U.)
Sp. Cond. (umhos/cm)
Waler Temp. (•c)
Odor (subjective)•
Turbidity {subjective)"
IS! Volume
«' /.. ,, ., "'
.,--, / -;,
2 I
' .
• (t)Hone (2)Slighl (3)Modcrale {4)Slronge
" (t)Clear (2)5lighlly lurbid {3)Moderalely Turbid
2nd Volume
/ ., 'I!,
/I-:<?
L-,-__s-'
,:,J
,!-I
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•
93
3rd Volume
• < ,<'
JI <<i
--s--
-.!
,. I
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(5)Exlremely Turbid
4th Volume 6th Volume
(SQU.f\lll)
t-t £ • d'd
D& r rorm4B (3/94)
fl.
-
DAJ.11S
FLffi:7D
CHCIHEERS
PLANNERS
ARCHIT[CTS
SCIEHflSlS
FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
CHARLESTON • G_RCCNWOOD • COLUMBIA -Well No · ,✓-:-,5-)-..
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crienl: C4/.d-/lq_/J_;tq_£_, T",t_ e.
Sile Name:Sbe/by, ,/2./C Job No.:/ //(75.,· I.
Date: 7 · /f · Z O C>o LWR submitted by: tlt.A.
Sampling Personnel: JLI-J 7 /w,,,-v
Site Personnel: ---Regulatory Personnel:
Weather Conditions: C'/4 c.:..drJ Temp.: <fl> ',5
Well Diameter: z. ~ In.
(A) Top of Well £1evalion: fJ" "3/(j_ l 't. msl {yes/no)
(B) Depth to Immiscible Layer. ·-ft.
(C) Immiscible layer Elevation: (A)-(B)= -msl (yes/no)
(D) Depth to Groundwater: :s: ::5'. r. 3 ft.
(E) Groundwater Elevation: (A)-(D)= r1 tJ, .5"t msl (yes/no)
(F) Total Well Depth = f-f"' !2---:: a tP fl.
{G) length of Waler Column: (F)-(0)= t!.~-3 7 fl.
Cosing Volume = (G) x Volume in gal./fl.= z, l. gals.
Method of Well Evacuation PL,. l:rJ p. Start lime: /I I!? 3
Method of Sample Collection ?'-'-1:2:U'> Time: /U--D
I
Chain-of-Custody Form Started ®/no)
Source(s) of Well ID M,:;ia I ID label (§Vno)
Well Completion: Protective Casing @/no) nush {yes@
Flush-Mount Cover Seal Intact (yes.(§) Locking Cap (yes~
Locked al Arrival (yes/:Ml Deparlure (yes/.ii>1
Well Casing {§ighl ab<i,/deplh below) ground: (...L-_,,?
Casing Type ~Steel) (Other) -
Dedicate~ or Bailer (yes/no) Type --
Protective Post/ Abulmentdy'.;,> no) Concrete Pad @/no)
Well Integrity Satisfactory (yes~ If no, explain below.
Well Yield & / moderate / high )
WELL VOLU~E DATA
DIA. OF PIPE (in.) VOLUME IN GAL/Ft.
1.0 0.041
2.0 0.163
3.0 0.367
4.0 0.653
5.0 .. 1.020
6.0 1.470
TO CONVERT GAL/Fl TO t.m:RS/FT. MULTIPLY ABOVE nGURES BY
3.8 LITERS/GALLON.
fl,
-
'
11
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FIELD ANALYSES .><-, A&_
6d'' 1 '
I
1st Volume 2nd Voll.Ina -1 ~ ,011,ue 4th Volume 6th Volumo
Volume Purged (gallons) 7. 7 1"2,1,/ ~ ,J_.,r-.~ I lime (military) , I , A // / "' 1 I ,::,'C
pH {S.U.) / J t,.O L , I
Sp. Cond. (umhos/ cm) z ,: ,,., z 1Jl> ;; 7 :,./ I Water Temp. ("C) 2 Z-:;, I i': I
Odor {subjeclive)• Q ,; ;f'
Turbidity {subjective)" ., '·-
• (1)Hone {2)Slighl (3)Moderole {4)Slronge I
" (1)cieor (2)Slighlly Turbid (3)Moderalely Turbid (4)Very Turbid (S)Exlremely Turbid
Commenls/Observolions/Recommendolions: ,/'~ /.('I,
-----------------•
-----------------------F-OR_M_C_O_M_PLCT_EO_C?=_·
__ J---c,/t'c;-X(--'&_l __ ,,--.E--·
"""""'I I ti : 7 -I i·"Q
O& F Form48 (3/94)
94 I
I
: ;f P."':::. :::: FIELD DATA LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
• Well No.: P-s-i.?
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crient: Cr(/d. /hl/,1tJ 5, :Z:n L qL /;;
Site Nome:Shefby, ,1\/C Job No.:/ llu'5., · '
Date: z·-l'f-zooc, LWR submitted by: _-.,.,,y"-"'4'-----
Sompling Personnel: J Lh /4¥4/
7
Sile Personnel: _____ -__________ _
--Regulatory Personnel: _____________ _
Weather Condilions:..;Cte:¼=.,._..=L,-~i--------Temp.:,Ro S:
Well Diameter: 2. ~ In.
(A) Top of Well Elevation: __ _,.7__./j"-"5'."-'. •c...l,._Z..=.. __ msl (yes/no)
(8) Depth to Immiscible Loyer: -fl.
(C) Immiscible Layer [levalion: (A)-(8)= -
(0) Depth to Groundwater: Z <f. f? F
msl (yes/no)
f I.
(E) Groundwater Elevation: (A)-(0)= 7-{ ? < z_ q msl (yes/no)
(F) Total Well Depth = _____ :z,-_,,s;.,_~,,,O...;.sO..e_ ___ __:.::ft.
(G) lenglh of Waler Column: (F)-(0)----~3"'-'.3"-.'-L' .,e::L~ __ f:.::t.
Cosing Volume = (G) x Volume in gol./ft.--__ ...;5c::.·--=•-4,___.:9..,,a""ls.
Method of Well Evacuation 'R,._b'.I p
Method of Sample tollection ?u. 01 I)
i
Chain-of-Custody Form Started ®/no)
Start Time: /? 3 •/
Time: ! ) 2 "
Source(s) ot Well 10 __ .,_M...u.a,._,f'CL.---ID label @'no)
Well Completion: Proteclive Cosing @/no) nush (yes@
nush-Mounl Cover Seal lnlocl (yes.(§} locking Cop (yes@!
Locked al Aniv~/no) Oepartur~o)
Well Cosing ~ighl ob0/deplh below) ground: 2-.S-fl.
Cosing Type (PVc)@other) ____ ~::--____ _
Dedicate~ or Boiler (yes/no) Type __ -____ _
Proteclive Post/Abutment (ye~ Concrete Pod @/no)
Well Integrity Solistaclory~no) It no, explain below.
Well Yield ( low / moderate /@)
WELL VOLUME DATA
DIA. Of PIPE (in.) VOLUME IN GAL/rt.
1.0 0.041
2.0 0.163
3.0 0.367
4.0 0.653
5.0 .. 1.020
6.0 t.470
TO CONVERT GAi/FT TO UTERS/FT, MULTIPLY ABOVE nGURES BY
3.B LITERS/GALLON.
-
FIELD ANALYSES
2nd Voltane ·~Id ~-dm,~
Volume Purged (gallon~)
Time (military)
pH (S.U.)
Sp. Cond. (umhos/cm)
Waler Temp. (•c)
Odor (subjective)•
Turbidity (subjective)"
1st Volume
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• (t)None (2)Slighl (3)Moderole (4)Slronge
" (!)Clear (2)Slightly Turbid (3)Moderolely Turbid
4th Volume 6th Volume
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(4)Very Turbid (5)Ex1remely Turbid
Comments/Observalions/Recommendolions: ____________________________
_
O& r rorm4B (3/94)
95
DfU/1S
FLtrfD
[HGIHEERS ARCHITtCTS
PLANNERS SCIEHHSIS
FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
CHARLESTON • C~t(HWOOO • COLUMBIA Well No ·C'-4-Cf -..
cnent: r' JJA-11'21'1.ttc.J:,,I">t.~ Source(s) of Well to M.a,, to Lobel @'no)
✓
I
Site Name:Sbelby, ,A(C Job No.:/ 1105.o ' Well Completion: Proleclive Casing @/no) nush (yes@
Ocie: 7 -(f Z Ooo LWR submitted by: 4'.-4 nush-tJounl Cover Seal Intact (yes.@ Locking Cop (yes@)
Sampling Personnel: JLM ,/;.(r4/ locked al Arrival ~no) Oeporlure <!i§}/no)
7
Site Personnel: -Well Cosing (feighl ob~/deplh below) ground: 3.., 0 fl,
Regulatory Personnel: Cosing Ty~ (Steel) (Other) -
Weather Conditions: C/4c..,.__) J Temp.:£> 5 Dedicate~ or Boiler (yes/no) Type -
Well Diameter. 2. ~ In-Protective Post/ Abulmen~/ no) Concrete Pod @/no)
(A) Top of Well [levalion: 'KG, ':L lL msl (yes/no) Well Integrity Solisfoclory~/no) If no, exploin below.
(B) Oeplh to Immiscible Loyer. -ft. Well Yield ( low / moderate / ~ )
(C) Immiscible Layer Elevation: (A)-(B)= -msl (yes/no)
(0) Oeplh to Groundwater. Z(. '-/i) ft. WELL VOLUME OATA
(E) Groundwater Elevation: (A)-(0)= f '/ Z, 7 / msl (yes/no)
OIA. or PIPE (in.) VOLUME IN GAL/rt.
1.0 0.041
(F) Total Well Depth = <I-9:. cu::J ft. 2.0 0.163
. (ii"'" 3.0 0.367
(G) length of Waler Column: (F)-(O)-27,{,0 ;z,/_~.,,-,,Pft. 4.0 0.653
5.0 .. 1.020
Cosing Volume = (G) x Volume in gol./ft.= q5"' gals. 6.0 1.470 -
Method of Well Evacuation p,_,._l:!J f2 Start Time: fr.:.o ~ TO CONVERT GAi/IT TO UTERS/n. MULTIPLY ABOVE nGURES BY
Method of Sample "Collection ?1.<-11:16 Time: I>/?
3.8 LITERS/GALLON.
I
Chain-of-Custody form Starled ®/no)
FIELD ANALYSES
1st Volume 2nd Votome 3rd Volume 4th Volume 6th Votumo
Volume Purged (gallon,) "./ q,o I -r-.s,-
Time (military) J,~,,,r ; ,-~L I. ,,_. '7 ,!./
pH (S.U.) _, --,, 1/. ,/ -.;_ ,,_/
Sp. Cond. (umhos/ cm) 111 / 7 17
Water Temp. (•c) I q J ii /,?
Odor {subjective)• ; I /
Turbidity (subjective)" I I I
• (t)None (2)Stighl (3)Moderole (4)Slronge
"{l)Cleor (2)Slightly Turbid {3)Moderolety Turbid {4)Very Turbid (S)Extremely Turbid
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Comments/Observolions/Recommcndalions: ------------------------------,
O& r form48 (3/94)
96
I
ID 1'}/1 S ENGINEERS ARCHITECTS FL6'i'D PLANHCRS SCl(HJISlS
FIELD DATA LOG
I CHARLESTON • C_REEHWOOD • COLUMBIA
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
Well No · j/ 1-1-7 7 ..
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er.en!: r' J/d-J/'2.lcp_ttos:_,, 01 "-Source(s) of Well ID Mia" ID Lobel {§Vno)
.J
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Sile Nome:Sb,./hy, ,AIC Job No.:/ 1!<750-1 Well Completion: Protective Casing @/no) Rush (yes@
Dole: Z • /~-zovo LWR submitted by: .!Pl-nush-t.lount Cover Seal Intact (yest§) locking Cap (yes@)
Sampling Pe~onnel: JLM 7 /Ma,/ locked al Arrivo~/no) Departure {.i;/no)
Site Personnel: Well Cosing (!i,ighl ob,0/deplh below) ground: c. ---;, fl.
Regulatory Personnel: Cosing Type (PVC)~!her) -
Wealher Condilions:C /4112 c: Ma1, Temp.: z'_c) Dedicate~ or Boiler (yes/no) Type -
Well Oiomeier: z_.,,.., In. Protective Post/Abutment (yes/<!!9} Concrete Pod @/no)
(A) Top of Well Elevation: 7.S-.J. vz msl (yes/no) Well Integrity Satisfactory ,ueA/no) If no, explain below.
(8) Depth lo Immiscible Loyer: -fl. Well Yield ( low / moderate / @)
(C) Immiscible Loyer Elevolion: (A)-(B)= -msl {yes/no)
(D) Depth lo Groundwater: L// Z3 fl. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(0)= ZI ,1, 6 </ msl (yes/no)
DIA. or PIPE (in.) VOLUME IN GAL/fl.
1.0 0.041
(f) Total Well Depth = 77 0 ° fl. 2.0 0.163
3.0 0.367
(G) Lenglh of Waler Calumn: (r)-(0)= ,}..S: 72 fl. 4.0 0.653
5.0 .. 1.020
Cosing Volume = (G) x Volume in gol./ft.= .> "7 6 gals. 6.0 1.470 -
Method of Well Evacuation p,.,__IZJ r-Start Time:/f'.;-:f TO CONVERT GAi/fl TO LITERS/fl, MULTIPLY ABOVE RGURES BY
Method of Sample "Collection p'-<-a!C! Time: JI J z..-
3.8 LITERS/GALLON.
I
Chain-of-Custody Form Started @/no)
FIELD ANALYSES
1SI Volume 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged (gallons) _j-. y I :z. I 11'"
Time (military) / ?/0 I? Z-, I l 3 c:l
pH (S.U.) -s--;l? /.: -0 r. 9
Sp. Cond. (umhos/ cm) 73 7.,J 7..,-
Waler Temp. ('C) ' 'ii / If'" 1F
Odor (subjective}• I J J
Turbidity (subjective)" I I )
• (t)Nonc (2)S!ighl (3)Moderole (4)Strongc
" (l)cteor (2)Slighlly Turbid (3)Moderolely Turbid ( 4)Very Turbid (5)Exlremely Turbid
Comments/Observolions/Recommendolions: -----------------------------
O& r rorm48 (3/94)
97
Df\VIS
FLtrfD
CHOIHEERS
PLANN(RS
ARCHIT[CTS FIELD DATA LOG
SCl(HHSIS FOR GROUNDWATER SAMPLE COLLECTION/
CHARLESTON • G,REEHWOOO • COLUMBIA GROUNDWATER ELEVATION MEASUREMENTS , ,
· Well No · J.I //---r 'i' -..
cr.ent: CA/d-//,,1,/t"Js,,ke.. Source(s) of Well 10 Man ID Lobel (§lino)
I
Sile Name:Sbelby, ,A.IC Job No.:/ 1105,o / Well Completion: Proleclive Casing (@/no) nush (yes.(®
Date: r· (l-\ · ZOoo LWR submilled by: -✓-V-#:. nush-Mounl Cover Seal lnlacl (yes.(§) Locking Cap (yes@)
Sampling Personnel: JLM 7 /MO,/ Locked at AJTivalg!f/no) Oeparlur~/no)
Sile Personnel: -Well Casing (!\eighl ab~/deplh below) ground: 2-.5---fl.
Regulatory Personnel: Casing Type (PVC)~Other) -
Weather Conditions: d4 c ,.-:;_1",.4 Temp.:-/ C> Dedicate~ or Bailer (yes/no) Type --
J
Well Diame·ler. z.,,.. In. Proleclive Posl/ Abulment (yes/~ Concrele Pad @/no)
(A) Top of Well [levation: 7 :r::G 1 '-{ msl (yes/no) Well Integrity Salisfoclory~/no) If no. explain below.
(B) Depth to Immiscible Layer: -fl. Well Yield ( low / moderate / high )
(c) Immiscible Loyer [tevalion: (A)-(B)= -ms! (yes/ no)
(0) Depth to Groundwater. ~l, 3 '.2 ft. W[LL VOLUME DATA
([) Groundwater Elevation: (A)-(0)= 719.11 msl (yes/no)
DIA. or PIP[ (in.) VOLUME IN GAL/n.
1.0 0.041
(F) Total Well Depth = t/r{. 0 d? ft. 2.0 0.163
t,t 7
3.0 0.367
(G) Lenglh of Waler Column: (F)-(0)= ft. 4.0 0.653
5.0 .. 1.020
Casing Volume = (G) x Volume in gal./ft.= I, {. gals. 6.0 1.470 -
Melhod of Well Evacuation pl,..= p. . Start Time: / ~~ </f TO CONVERT GAL/FT TO LITERS/FT. MULTIPLY ABOVE nGURES BY
Method of Sample ·collection ?«.mCl Time: /t !J 3.8 LITERS/GALLON.
I
Chain-of-Custody Form Storied @/no)
FIELD ANALYSES {~
1st Volume 2nd Volume 3rd Volume --4t•1 'i O'OIIIB 6th Volume
Volume Purged (gallons) J I 2. l, nfJ ,,-;o ;z " -
Time (military) , e.s'_,,. I,--r .;;, ~ ... ,.,, 1:f-$1-~•I.~ -
pH (S.U.) ;::-:.1 s-: z_ >-=-.3
Sp. Cond. (umhos/cm) ... ~, ..ro <./4
Waler Temp. (•c) / :,r /',f I I?
Odor (subjective)• , I I
Turbidity {subieclive)•• , I 1
• (t)None (2)Slighl (3)Modero!e (4)S!ronge
" (t)cteor (2)Slighlly Turbid (3)Moderolety Turbid (4)V~ry Turbid (5)Exlremely Turbid
Comments/Observalions/Recommendalions: -----------------------------
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98
FORM COMPL[T[Ol ~"",~C.,,....Ji.~~!f:'.'.t!!..!"ib~ ..1?.:
;,--~u.=::____ __ =-,
O& r rorm48 (3/94)
I
I
I DFLJUIIDS [NGIN[ERS ARCHIT[CTS Lfil° PLANHCRS SCl[HJISIS
FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS T-__, I CHARLESTON • G,RCENWOOO • COLUMBIA . · WellNo· --~c.5 ..
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Client: r' 41.d.. J/L:t.~!IO~, Z:,.,L Source(s) of Well ID M.aa ID label ®'no)
h .., I
Sife Name:,S],e / [' ,A[ C Job No.:/ I /(75, 0 r Well Completion: Protective Cosing @/no) Rush (yes@
Oafe: Z ·[ '1,-ZOoc, LWR submilled by: .llll flush-lJounl Cover Seal Intact (yesl§} Locking Cop (yes~
Sampling Personnel: JLtJ lw,Gv'. lacked at Arrival/fi)/no) Oeparlure ~~no)
l Well Casing (§"ighl ab~/depth below) ground: -
Site Personnel: -3 _::, (I,
Regulatory Personnel: -Casing Type (PVC~) (Ofher) -
Weather Conditions: C/,-,ac Temp.: -1615 0cdica1e~ or Boiler (yes/no) Type --
Well Diameier: z_.,.., In. Proleclive Posi/ Abutment (yes/ no) Concrete Pad @/no)
(A) Top of Well [levation: 7 7?:,,l.? ms! (yes/no) Well lnlegrity Salisfo~/no) If no, explain below.
(B) Oeplh lo Immiscible Layer. -fl. Well Yield ( low / era / high )
(C) Immiscible layer [levalion: (A)-(B)= -msl (yes/no)
(0) Depth to Groundwater. I z z C. fl. W[Ll VOLUI.I[ DATA
(E) Groundwater [levation: (A)-(0)= 7G -<,,t Z. msl (yes/no)
DIA. or PIP[ (in.) VOLUM[ IN GAL/rt.
1.0 0.041
(f) Toto! Well Oepth = :rs:.,_ ft. 2.0 0.163
c 5-:/i
3.0 0.367
(G) Length of Water Column: (F)-(0)= ft. 4.0 0.653
5.0 .. 1.020
Cosing Volume = (G) x Volume in gol./ft.= .3, :Fi gols. 6.0 t.470 -
Method of Well Evacuation 'R..m p Storl Time:/ t.' 5 0 TO CONV[RT GAl/fT TO LITERS/FT. MULTIPLY ABOV[ RGURES BY
3.8 LITERS/GALLON.
Method of Sample Collection Pt.<.1:210 Time: 17 7 0
I
Chain-of-Custody form Storied ®/no)
FIELD ANALYSES f":::'Jo/4
1st Volume 2nd Volume Scd Volume Alb ~'eh:lme 6th Volume
Volume Purged (gallons) ✓, Jl 7, /. D~Y, 2 ~ ... ,. --. .
Time (military) 17-✓I / 7/ )' -
pH (S.U.) " Z---:-1 ..-:. ;i,.
Sp. Cond. (umhos/cm) LlL.!(j // (/ & <Jdf
Water Temp. (•c) / q /,; /4
Odor (subjective)• J I I
Turbidity (subjective) .. ,. I I
• (t)Hone (2)Slight (3)Moderate (4)Stronge
" (1)Ctear (2)Slightly Turbid (3)Moderalety Turbid (4)Very Turbid (5)£xtremety Turbid
Comments/Observations/Recommendations: -----------------------------
D& r ro,m48 (3/94)
99
D1\)11S
FLfil'D
[NGIH((RS ARCHITECTS
PLANH(RS SCl(Hflsrs
FIELD DATA LOG
I
I
CHARLESTON • C_Rl:EHwooo • COLUMBIA
Client: C,r/.A-Jh/J djS,, .I,, "-
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
-Well
Man
.. No·//--; 3 cf I
Source(,) of Well ID ID label e'no) I
Site Name:Sbelby, /,IC Job No.:/ J!Cl.S:0~1 Well Completion: ProlecHve Cosing (@/no) nush (yes@
Date: Z -/ £· Z Ooc, LWR submitted by: /v'A-nush-1.Aounl Cover Seal Intact (yes/§) Locking Ccp (yesh!!l)
' Departurtfr"--;)o)
Sampling Personnel: JLM lwn/ locked at Anival~/no)
I
Sile Personnel: ~ Well Casing (feighl ab<0/deplh below) ground: 2-d f!.
Regulatory Personnel: Casing Type (PVC~lher) -
Weather Conditions: c/4,,_ K
I Dedicate~ or Bailer Temp.: '.z72 j (yes/no) Type -
Well Diameier. z_,,.., In. Protective Post/ Abutment (yes/ii»P Concrete Pad @/no)
(A) Top of Well [tevation: 77z. 73 msl (yes/no) Well Integrity Satisfactory tf£"/no) If no, explain below.
(B) Depth lo Immiscible Layer. -ft. Well Yield ~ moderate / high )
{C) Immiscible Layer Devalion: (A)-(B)= -ms! (yes/ no)
(D) Depth to Groundwater. I 7,. z c. ft. W[LL VOLUME DATA
(E) Groundwater Elevation: (A)-(0)= 7 6 O, i7 msl (yes/no) DIA. or PIPE (In.) VOLUME IN GAL/Ft.
1.0 0.041
(F) Total Well Oepth = 1 ¼.) fl. 2-0 0.163
? "-/ ft.
3.0 0.367
(G) Length of Water Column: (F)-(0)= ? ?. 4.0 0.653
5.0 .. 1.020
Casing Volume = (G) x Volume in gol./ ft.= r~ got,_ 6.0 1.470
Start Time: 111 -{
-
Method of Well Evacuation PL<-b:J. p TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOV[ nGURES BY
Method of Sample totlection ?t<.azD nme/,f?,~
3.8 LITERS/GALLON.
I
Chain-of-Custody Form Storied @/no)
FIELD ANALYSES ~ 1st Volume 2nd Vok.ane 3rd Volume 6th Volume
Volume Purged (gallons) 7, / ]>IDV( a) / <i_. -
Time (mmtary) /7do /75(,
__,
pH (S.U_) .:-, 7 .,,.._ ~ J. 1
Sp. Cond. (umhos/cm) #8' ¥= ,, -4
Waler Temp. ('C) J "1 I 7 I -,
Odor (subjective)• I I I
Turbidity (subjective)" I
I .
• (t)None (2)Slighl (3)Moderole (4)Slronge
" (t)Cleor (2)Slightly Turbid (3)Moderalely Turbid (4)Very Turbid (5)Exlremely Turbid
Comments/Observolions/Recommendolions: ------------------------------
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------------------rf----t---t--1
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ID 1'}/1 S [NCIHHRS ARCHff[CTS
FLG'l:D Pl.A.NN(RS SCJEHHSJS
FIELD DAT A LOG
I CHARLESTON • G_REEHWOOD • COLUMBIA
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
Well No • /"),.::: {;' z__ ..
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Client: f'7 J/.d.. J/,z./cp_do.f, :Z:>1.i!. Source(s) ot Well ID Maa ID label C§,'no)
.,,-, I
Site Hame:Sbe / b T, /,,IC Job Ho.: / I IO'S. 0 • ' Well Completion: Proleclive C<ising @/no) flush (yes@
Dale: 7 ·/1· ZOoc, LWR submilled by: #If nush-lJounl Cover Seal Intact {yesl§} Locking C<ip {yes@)
Sampling Personnel: JLtJ 7 ,/w,,:-4/ Locked at Arrival~no) Oeparlur~no)
Site Personnel: ----Well Casing (!i,ighl ab~/deplh below) ground: 2. Z> II, -Casing Type {PVC) ~Q (Other)
Regulatory Personnel:
-
Wealher C<indilions: c/4.,,., Temp.: 9o.) Dedicate~ or Bailer (yes/no) Type -
Well Diameter. z.~ In. Protective Post/ Abulmenl (yes/:fft:i Concrete Pad @/no)
(A) Top of Well Elevation: zz,z.1.f.. msl (yes/no) Well Integrity Salistaclory ~no) It no, explain below.
(B) Depth to Immiscible Layer: -It. Well Yield @! moderate / high )
(C) Immiscible layer Elevation: (A)-(B)= -msl (yes/no)
(0) Oeplh to Groundwater: l 2, 4.{ It. WELL VOLUME DATA
([) Groundwater Elevation: (A)-(O)-73;q ,7 ?f mst (yes/no)
DIA. or PIPE (in.) VOLUME IH GAL/fl.
1.0 0.041
(f) Tolol Well Oeplh = ~ ,z. L/o II. 2.0 0.163
L/t/. 7 1 3.0 0.367
(G) Lenglh of Water C,,lumn: (f)-(0)= fl. 4.0 0.653
5.0 .. 1.020
Casing Volume = {G) x Volume in gal./fl.= f'.z. gals. 6.0 1.470 .
Melhod · of Well Evacuation pl,.tt, p. Slarl Time:/ z s' 7 TO CONVERT GAL/fT TO LITERS/fr, MULTIPLY ABOVE flGURES BY
Method of Sample tolleclion Pt.c..at/) Time: / Z J .>-
3.8 LITERS/GALLON.
I
Choin-o!-Cuslody form Started @/no)
FIELD ANALYSES S< /} . /
1st Volume 2nd Volume 3rd Volume 4th Yofume 6th Volume
Volume Purged {gallons) S'. ?. . /, 4 V l> .,
Time {moilary) It?/ .3 I -v , I -
pH {S.U.) .::,-5,;·,;, <a-; s? s-; 7
Sp. Cond. (umhos/cm) / 0 L I /. I
Waler Temp. (•c) /..,,.. /~ ,~
Odor {subjective)• J I (
Turbidity (subjective)" I I I
• (1)Hone (2)Slighl (3)Moderole (4)Slronge
" (l}clear (2)Slightly Turbid (3)Moderolely Turbid (4)i'ery Turbid (5)Exlremely Turbid
Comments/Observotions/Recommendalions: ------------------------------
Ok r form48 (3/94)
1 01
Df\l!IS
FL6YD
CHCIHEERS
PLANNERS
ARCHITECTS FIELD DAT A LOG
SCIEHHStS FOR GROUNDWATER SAMPLE COLLECTION/ '[) L-\ p
.CHARLESTON • G.RCENWOOO • COLUMBIA GROUNDWATER ELEVATION MEASUREMENTS
Well No ,t;-c-c L -
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Client: f" J/d.-1/;z.~dq_,f ,fl'J."-Source(s) of Well ID Maa ID Lobel @'no)
,/ , I
Sile Name: fbe 1/,y/ ,6.1 C Job No.:/ //(75, o~' Well Completion: Proleclive Casing @/no) Rush (yes@
Cafe: 7 · {J· ZOoo LWR submilted by: ,41..&! nush-Mounl Cover Seal Intact (yes.(§) Locking Cap (yes~
Sampling Personnel: JLtJ 7 ih-YA-<'. Locked al Arrival (yes/no) Departure (yes/no)
Site Personnel: -Well Casing (&ighl ab~/deplh below) ground: 2---'> fl,
Regulatory Personnel: Casing Type (PVC)~)(Other) -
Wealher Candilions: c/4., C
,
Dedicate~ or Bailer Temp.: <115 ,I (yes/no) Type -
Well Oiameier. z_.,-., In. Proleclive Post/ Abulmenl (yes/§) Concrele Pad @/no)
(A) Top of Well [levotion: 711-7-;y msl (yes/no) Well lnlegrity Salisfaclory<l@/no) If no, explain below.
(B) Depth to Immiscible Layer. -ft. Well Yield ( low / moderate / ~
(C) Immiscible Loyer Elevation: (A)·(B)= -msl (yes/no)
(D) Depth to Groundwaler. If.~~-fl. WELL VOLUME DATA
(E) Groundwoler Elevation: (A)·(O)= 7 5 / // ( msl (yes/no)
DIA. or PIPE (in.) VOLUME IN GAL/fl.
1.0 0.041
(f) Tolol Well Oeplh = ~ 1-0 fl. 2.0 0.163
3.0 0.367
(G) Lenglh of Water Column: (r)-(0)= ij/ Jd' ft. 4.0 0.653
5_0 .. 1.020
Casing Volume = (G) x Volume in gol./ft.= t.1 gals. 6.0 1.470 -
Method of Well Evacualion Pv-tn p. Start Time: 115-'i/ TO CONVERT GAi/FT TO UTERS/fT, MULTIPLY ABOVE RGURES BY
Method of Sample ·eonection ?L<.l1::!l:! Time:/£ I> 3.8 LITERS/GALLON.
I
Chain-of-Custody form Slar1ed @/no)
FIELD ANALYSES '))«p
1st Volume 2nd Volume 3rd Volume -tth Yela111e 6th Volume
Volume Purged (gallon~) t.7 I 1. ;/ 2-t?. -, -
Time (mililary) Q ~ l/-I '114 , ~ ..1 I -✓,;:fi 1
pH (S.U.) , ' I. I j , / 6, I
Sp. Cond. (um hos/ cm) ~ r; { 7 If ~c I Waler Temp. (•c) t/2 , 7 I 7 /?
Odor (subjeclive)• I ' I 1
Turbidity (subjeclive)" I , , I
• (1)None (2)Slighl (3)Moderale (4)Slronge I
" (1)Clear (2)Slightly Turbid (3)Moderalely Turbid (4)Very Turbid (5)Exlremely Turbid
Comments/Observolions/Recommendalions: ----------------------------1
O& f form48 (3/94)
102 I
I
1D1'}11S [HGIH[[RS ARCHITLCTS
FLffi'D fl.ANH(RS SCIEHJISIS
FIELD DAT A LOG
I CHARLESTON • G_REENWOOD • COLUMBIA
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
-Well No · A-/1-S-J ..
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Cfienl: f" J).1._. J/,z/Jdtz,'£,, ':£>1.i!_ Source(s) of Well to Maa to Lobel @'no)
Sile Hame:Sbe/hy, 1,/C Job Ho.:/ 110'5.o '
I
Well Completion: Proleclive Casing @/no) flush (yes@
Dale: 7 ·/9-ZOoc, LWR submilted by: 4/fi nush-l.lounl Cover Seal Intact (yes,{§) Locking Cap (yes~
Sampling Personnel: JLM !.~.<:::. Locked al Arrival &5Yno) Departure GYno)
7 -
Site Personnel: --Well Casing ~ighl ab0/deplh below) ground: /4 j (I, -"""'
Regulatory Personnel: Casing Type (PVC) ~') (Other) -
Weather Candilions: ('.;/-Gd< ~( Dedicale~ or Bailer (yes/no) Type Temp.: J· j -
Well Oiameier: z_,,.., In. Protective Post/Abulmenl (yes/~J Concrete Pad @/no)
(A) Top of Well Elevation: 'l 1?i 1, msl (yes/no) Well lnlegrily Salisfoctory@no) If no, explain below.
(8) Depth to Immiscible Layer: -fl. Well Yield ( low /~ high )
{C) Immiscible Loyer Elevation: (A)-(B)--' -msl {yes/no)
(D) Depth lo Groundwater: ) >. 21: fl. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(D)= ] f'. / , f O msl (yes/no)
DIA. or PIPE (in.) VOLUME IN GAL/Ft.
1.0 0.041
(F) Total Well Depth = ,5 ~ ,:?,:;> fl. 2.0 0.163
t:.t.-24
3.0 0,367
(G) Length of Waler Column: (F)-(D)= ft. 4.0 0.653
I 5.0 .. 1.020
Casing Volume = (G) x Volume in gal./11.= 5. 0 gals. 6.0 1.470 -
Method of Well Evocuofion PL,,.123 f!. Slort Time: /f'l/-:Z.,. TO CONVERT GAi/FT TO lJT£RS/FT. MULTIPLY ABOVE flGURES BY
Uethod of Sample "Collection ? "'-aU'> Time: 1-,:, .,, 8'
3.8 LJT£RS/GALLON.
I
Chain-of-Custody Form Storied ®/no)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged {gollons) .\,o ,, • e? q, ,.,
Time (mmtary) ,,.7 ,,_.._, , ,i.5 r "t)O"
pH (S.U.) -4!7 ,, I 7 4. 7
Sp. Cond. (umhos/cm) ,,.-,z iv-Z 8<>
Woler Temp. {°C) // /L /t{
Odor (subjective)• ; I I
Turbidily (subieclive)" I J ,
• (l)None (2)Slighl (3)Moderole (4)Slronge
" (l)Cteor (2)Slighlly Turbid (3)Moderalely Turbid (4)Very Turbid (5)Exlremely Turbid
Comments/Observotions/Recommendolions: ------------------------------
FORM COMPLETED
D& r rorm'B (3/94)
103
Df\VIS
FL6\7D
CHCIHECRS
PLANNERS
ARCHffECTS
SCIEHflSlS
FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
CHARLESTON • G_R£ENWOOO • COLUMBIA Well No • I!, z_ 'i? -.. -
Client: /" J/J._. J/,:./J_t:1q_~, Z",z "-Source(s) of Well to Mcaa to label @'no)
./ , I
Site Nome:Sbefh 1, ,t,.!C Job No.:/ //(75,.-/_ Well Complelion: Protective Casing @/no) Flush (yes@
Oofe: Z -[9.-ZOoc, LWR submitted by: l}IA nush-Mounl Cover Seal Intact (yes@ Locking Cap (yes~
Sampling Personnel: JLlj
7 /4-YJ<,( lacked of Arrivol~/no) Oeporlure@/no)
Site Personnel: ---Well Cosing (!i;ighl ob~/deplh below) ground: L/.E) ft,
Casing Type (PVC) ~ (Other)
Regulatory Personnel:
-
C/6'0.:::: ~~1 Temp.: {1~ ~ Dedicate~ or Bailer (yes/no) Type -
Weolher Conditions:
Well Oiomefer: z_~ In. Protective Post/Abutment ~no) Concrete Pod @/no)
(A) Top of Well Elevation: 'Z.t l, zo msl (yes/no) Well Integrity Salisfaclory~/no) If no, explain below.
(8) Oeplh fo Immiscible Layer. -fl. Well Yield @; moderate / high )
(C) Immiscible Layer Elevation: (A)-(8)= -msl (yes/no)
(D) Depth lo Groundwofer. 'Zi• ZG fl. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(D)= Zil't',14 msl (yes/no) DIA. or PIPE (in.) VOLUME IN GAL/fl.
1.0 0.041
(F) Total Well Deplh = '2 'fl,,90 fl. 2.0 0.163
t. zd
3.0 0.367
(G) Length of Waler Column: (F)-(D)= fl. 4.0 0.653
5.0 .. 1.020
Casing Volume = (G) x Volume in gal./ft.= LL gals. 6.0 1.470 .
Method of Well Evocuafion Pt,..1::n p. Slarl Time: z,£f_ TO CONVERT GAi/fl TO LITERS/IT, MULTIPLY ABOVE FlGURES BY
Method of Sample 'collection ?1..t.a:U'> Time: ? i) ccJ 3.B UTERS/GALLON.
I
Chain-of-Custody Form Storied (@/no)
FIELD ANALYSES 5~
1st Volume 2nd Volume 3rd Volume --4th ffolcnne 6th Volume
Volume Purged (gallon,) /. I ;, . ~ hll' •Al ....,, • -
TTme (military) lo,, '7,t)J >
pH (S.U.) / _, /.. ;) 6.;
Sp. Cond. (umhos/ cm) z,;-.d ,, ,-,I-~ <"C,
Waler Temp. (•c) /,? I ii'" t&'
Odor (subieclive)• z -> ?
Turbidity (subjective)" I I I
• (t)Hone (2)Slighl (3)Moderale ( 4)Slronge
" (t)ctear (2)Slighlly Turbid (3)Moderalely Turbid (4)Very Turbid (5)Exlremely Turbid
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Comments/Observolions/Recommendolions: ------------------------------1 I
O& r rorm48 (3/94)
104
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I D 1'}/1 S [HGIH[(RS ARCHITI:CTS FL6f"D PLANNERS SCtEHflSTS
FIELD DAT A LOG
I CHARLESTON • G,REENWOOO • COLUMBIA
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWA TEA ELEVATION MEASUREMENTS
. Well No· V-Z-3 ..
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Client: CJ.Ld.-1/,:.~dQ~, £;i"-Source(,) ol Well ID M.a,, ID Lobel @'no)
./ , I
Site Name: fbelby, ,A(C Job No.:I"' 11<7.5 I Well Complelion: Proleclive Cosing (@/no) nush (yes@
Date: 7 · !'f-Z O <!:>D LWR submilled by: /1/A-'
nush-Mount Cover Seal Intact (yesl§} Locking Cop {yes~
Sampling Personnel: JLIJ 7 1/4//Jr,( locked at Arrival rti.),/no) Deparlure (ii't;/no)
Site Personnel: Well Cosing ~ight aboft/depth below) ground: $. c) II,
Regulatory Personnel: -Cosing Type {PVC) ~ (Other) -
Weolher Conditions: CLe12. c. Temp.:© S Dedicate~ or Bailer (yes/no) Type -
Well Oiomeier. z_,.,., In. Protective Post/ Abutment (yes/§ Concrete Pod @/no)
(A) Top of Well Elevation: 1? l l. ~'j msl (yes/no) Well Integrity Satisloctory <f0/no) II no, explain below.
{B) Depth to Immiscible Loyer: -It. Well Yield ( tow / moderate / @l
(C) Immiscible Loyer [levolion: (A)-(B)= -ms! (yes/no)
{D) Depth to Groundwater: l 7, 1 LI It. WELL VOLUME DATA
(E) Groundwater Elevation: {A)-(D)= ] 9 ,j , 1 Omsl (yes/no)
0IA. or PIPE (in.) VOLUME IN GAL/fl.
1.0 0.041
(f) Total Well Depth = z 3', 4 ft. 2.0 0.163
3.0 0.367
(G) Length of Water Column: (f)-(D)= s-:tJ t ft. 4.0 0.653
5.0 ,. 1.020
Cosing Volume = {G) x Volume in gat./ft.= (., 0 gals. 6.0 1.470 .
Method of Well Evacuation Pc..1'?:l fJ-Start Time: z c, z 1. TO CONVERT GAi/fl TO UTfRS/fT, MULTIPLY ABOVE flGURES BY
Method of Sample Collection ?u. 1:21 Cl Time: "O'z'z": 3.8 UTfRS/GALL0N.
I
Chain-of-Custody form Storied (@/no) .
FIELD . ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged (gallons) I ,O :,,,-.o l,"'
Time { mililory) """""' J
lo ? 5 2 O·' ,f
pH (S.U.) 4':lfl .f,-r, ,-; /)
Sp. Cond. (umhos/cm) L (7 f' ,,.-, :,t; l'~ .5rq I 0
Water Temp. ("C) / -r I i;.> I "8
Odor (subjective)• -r ;,-c
Turbidity {subjective)"" J I I
• (!)None (2)Slight (3)Moderote (4)Slronge
" (!)Clear {2)Slighlly Turbid (3)Moderotely Turbid (4)Very Turbid (5)Exlremely Turbid
Comments/Observolions/Recommendations: ------------------------------
FORM COMPlIT[,9-D ~~z!;'.;.-4~~;f.-µ,¥,~:!:f~
0
0& F Form48 (3/94)
105
DAYIS
FLtwD LABORATORY ANALYSIS REPORT
Explanation of Symbols and Abbreviations
The following defines common symbols and abbreviations used in reporting technical data:
RDL Report Detection Limit MDL Method Detection Limit
TOP Top of Pipe MSL Mean Sea Level
TNTC Too Numerous To Count MPN Most Probable Number
BTU British Thermal Units NTU Nephelometric Turbidity Units
C Degrees Centigrade F Degrees Fahrenheit
umhos/cm micromhos/cm meq milliequivalents
kg kilogram(s) g gram(s)
mg milligram(s) ug microgram(s)
I liter(s) ml milliliters(s)
ul microliter(s) m3 cubic meter(s)
lb pound(s) ft3 cubic foot(feet)
ft foot(feet) TIC Tentatively Identified Compounds
mg/I, mg/kg Units of concentration in milligrams per liter for liquids and milligrams per kilogram for solids. Also
referred to as Parts Per Million or "ppm" when the assumption is made that the specific gravity or
density is one (1 g/ml).
ug/1, ug/kg Units of concentration in micrograms per liter for liquids and micrograms per kilograms for solids.
Also referred to as Parts Per Billion or "ppb" when the assumption is made that the specific gravity
or density is one (1 g/ml).
wt%
<
>
Units of concentration expressed on a weighUweight basis (e.g. grams per 100 grams).
Less Than -The number following the sign is the limit of quantitation, the smallest amount of
analyte that can be reliably determined using this test.
Greater Than
Data Qualifiers:
A
B
C
E
J
p
X
*
TIC is a possible aldol-condensation product resulting from sample extraction, (Organics)
Analyte also detected in the method blank.
Amendable Cyanide is a negative value due to an unknown interference.
Estimated concentration due to interference.
Estimated value below RDL or estimated value for TIC. (Organics)
Concentration difference between primary and confirmation columns >25%. (Organics) The lower result is
reported.
Matrix interference which requires dilution or prevents the reporting of a result. Detection limits have been
adjusted where applicable.
Defined in report comments.
Solid samples (i.e. soil, sludge, and solid waste) are reported on a dry weight basis unless otherwise noted.
Test results relate only to the sample tested. Clients should be aware that a critical step in a chemical or biological
analysis is the collection of the sample. Unless the sample analyzed is truly representative of the bulk of the material
involved, the test results will be meaningless. If you have any questions regarding the proper techniques of collecting
samples, please contact us. However, we cannot be held responsible for sample integrity unless sampling has been
performed by a member of our staff. ·
WARRANTY AND LIMITATION OF LIABILITY -The accuracy of all analytical results is warranted for the sample as
it is received by the laboratory. Warranty for the integrity of the sample begins at the time it is placed in the
possession of authorized Davis & Floyd, Inc. Laboratories personnel. All other warranties, expressed or implied, are
disclaimed. Liability is limited to the cost of the analysis.
Davis & Floyd, Inc.
AD07_0/ (07199)
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Davis & Floyd, Inc. I PO Drawer 428 ) Greenwood, SC 29648 I <316
1
EQD6rst t\venue I Greenwood, SC 29649 I [phone] I F;1x (H64) 22'.l-71 ! YI
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DATA ASSESSMENT SUMMARY CHECKLIST AND REPORT -LEVEL II
Client ID:
Project Number:
Monitoring period:
CNA Holdings. Inc.-Shelby
TF026DB01
04/00
Sample Delivery Group (SDG) Description:
Prepared By: Diane M. Rosseter
Date: 12/21/00
Quarterly monitoring well samples collected and analyzed by Davis & Floyd, Inc. of Greenwood.
SC for volatiles, ethylene glycol. and total organic carbon according to EPA/SCDHEC approved
methodolo!!v
CONTENTS LEVEL COMMENTS
II
Sample Results -All data Class A except as noted in
the discussion section below.
Method Conformance Summary -O.K.
Chain(s) of Custody (COCs) -Various info incomplete. No effect
on data.
Master Tracking List -O.K.
Case Narrative
Sample Prep
Standards Prep
Instrument Quality Control Data
Batch Quality Control Report -O.K.
Surrogate Recovery Report
Trip/Field/Equipment Blank Report -O.K.
Field Notes/Logbook -O.K.
CLP Forms
All Raw Data
Electronic Deliverables -O.K.
Discussion:
I . Acetone and 2-butanone were detected in the trip blank. Positive results for acetone and 2-
butanone in the associated samples at levels less than IO times that found in the trip blank
were flagged with "U" and the reporting limit raised to the concentration of acetone or 2-
butanone present in the sample. The only associated sample containing acetone or 2-
butanone was ITC!. Results for these compounds in ITC! were flagged as indicated above.
Kubal-Furr & Associates
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26OB0! -Q4/00 DAS -

2

-
12/21/00
2. The relative percent difference between the K-28 and the field duplicate K-28 Dup. was
outside acceptance criteria for TOC. Results for TOC in K-28 and K-28 Dup. were flagged
with "J".
J = positively identified, however concentration is estimated
U = not detected at the associated sample quantitation limit
Class A = quantitative Class B = qualitative
Kubal-Furr & Associates
Class C = unusable
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,., -r"-er u u
/2e L' ( se~<1 J) /)-f•-
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
November 28, 2000
JERRY MCMURRAY
TICONA, LLC
PO BOX 87
SHELBY, NC 28150
Login Number
Project Number
Description
:L00102603
:61195.00-0004
:WELL SAMPLING
Dear Jerry Mcmurray:
We are pleased to provide the enclosed analytical results for the samples received by
Davis & Floyd, Inc. on October 25, 2000.
A formal Quality Assurance/Quality Control program is maintained by Davis & Floyd,
which is designed to meet or exceed the EPA or appropriate regulatory requirements.
All analytical analyses for this project met QA/QC criteria unless otherwise stated in the
footnotes. This report is to be reproduced only in fulL
Feel free to contact our Client Services Representative at [phone] if further
explanation of the analysis is required. Unless other arrangements have been made, samples
will be disposed of or returned 14 days from the date of the report. We appreciate the
opportunity to provide services to your firm.
Sincerely,
DAVIS & FLOYD, C.
~
ohn H. McCord, Jr,
Laboratory Manager
I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
1
Df\YIS
FLtJ\'D LABORATORY ANALYSIS REPORT
Client
Contact
TICONA, LLC
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITEF
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 90408
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Gao Chromatography
SW846 8015
ETHYLENE GLYCOL
Volatile Organics
SW846 82608
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANQNE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
OIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
GW/ChemW
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
Result
21.0
8. 2
3200
NA
7.0
0. 0050
0 .0050
0. 0050
0 .0050
0 .0050
0 .0050
0. 0050
0 .010
0. 010
0.0050
0. 010
0. 0050
o. 0050
0. 0050
0.010
0 -0050
0 . 0050
0 . 0050
0. 010
0.0050
0.010
0.0050
0 . 0050
0 .0050
0 .0050
0 . 0050
Project Number: 61195.00-0004
Report Date
Page 1 of 2
November 28, 2000
Sample ID L00102603-01
Date Collected: 25-0CT-00 12:56
Date Received
Qual Units Analyst Date Time
1.0 degrees C 10/25/00 1256
0.50 SU 10/25/00 1256
1.0 umhos/cm 10/25/00 1256
. 01 feet MSL 10/25/00 1256
7.0 JMT 10/31/00 2240
0 .0050 mg/1 PAP 10/31/00 1303
o. 0050 mg/1 PAP 10/31/00 1303
0 .0050 mg/1 PAP 10/31/00 1303
0 . 0050 mg/1 PAP 10/31/00 1303
0 .0050 mg/1 PAP 10/31/00 1303
o. 0050 mg/1 PAP 10/31/00 1303
0.0050 mg/1 PAP 10/31/00 1303
0.010 mg/1 PAP 10/31/00 1303
0.010 mg/1 PAP 10/31/00 1303
0.0050 mg/1 PAP 10/31/00 1303
0. 010 mg/1 PAP 10/31/00 1303
0 . 0050 mg/1 PAP 10/31/00 1303
0.0050 mg/1 PAP 10/31/00 13 03
0.0050 mg/1 PAP 10/31/00 1303
0.010 mg/1 PAP 10/31/00 1303
0 .0050 mg/1 PAP 10/31/00 1303
o. 0050 mg/1 PAP 10/31/00 1303
0 .0050 mg/1 PAP 10/31/00 1303
0.010 mg/1 PAP 10/31/00 1303
0.0050 mg/1 PAP 10/31/00 1303
0.010 mg/1 PAP 10/31/00 1303
0 .0050 mg/1 PAP 10/31/00 1303
0 .0050 mg/1 PAP 10/31/00 1303
0 .0050 mg/1 PAP 10/31/00 1303
0.0050 mg/1 PAP 10/31/00 1303
0.0050 mg/1 PAP 10/31/00 1303
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 l [phone] 1 Fax [phone]
2
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
T:tCONA, LLC
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITEF
Parameter
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE {TOTAL)
Wet Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
Result
< 0 . 0050
< 0. 0050
< 0 . 0050
< 0. 0050
< 0 .0050
< 0. 0050
< 0 .010
< 0 .010
< 0.0050
25.9
Project Number: 61195.00-0004
Report Date November 28, 2000
Page 2 of 2
Sample ID L00102603-0l
Qual RDL Units Analyst Date Time
0 .0050 mg/1 PAP 10/31/00 1303
0 .0050 mg/1 PAP 10/31/DO 1303
0. 0050 mg/1 PAP 10/31/00 1303
o. 0050 rne/1 PAP 10/31/00 1303
0.0050 mg/1 PAP 10/31/00 1303
0.0050 mg/1 PAP 10/31/00 1303
o. 010 mg/1 PAP 10/31/00 1303
0 .010 mg/1 PAP 10/31/00 1303
0.0050 mg/1 PAP 10/31/00 1303
1.0 mg/1 TRB 11/02/00 1428
I Davis & Floyd, Inc. \ PO Drawer 428 I Greenwood, SC 29648 \ 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]l l 9
3
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA, LLC
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITCI
Parameter
Field Data
EPA 170.l
TEMPERATURE
SW846 904GB
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Gas Chromatography
SW846 8015
ETHYLENE GLYCOL
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETJ-W,./E
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
GW/ChemW
Result
21. 0
S. 2
1250
NA
779
< 0. 010
< 0 .010
< 0 .010
< 0 .010
' 0 .010
< 0 . 010
' 0 .010
0.021
< 0.020
' 0. 010
0.20
0.013
' 0. 010
' 0 .010
' 0 . 020
< 0. 010
' 0 .010
0,013
' 0 .020
' 0. 010
' 0.020
' 0. 010
' 0. 010
' 0. 010
' 0. 010
' 0 .010
Project Number; 61195.00-0004
Report Date November 2 B, 2 000
Page 1 of 2
sample ID L00102603-02
Date Collected, 25-0CT-00 13 :08
Date Received 25-OCT 00
Qual RDL Units Analyst Date Time
1.0 degrees c 10/25/00 1308
0.50 SU 10/25/00 1308
1.0 umhos/cm 10/25/00 1308
.01 feet MSL 10/25/00 1308
35.0 mg/1 JMT 11/01/00 1740
X o. 010 mg/1 PAP 10/31/00 1328
X 0 .010 mg/1 PAP 10/31/00 1328
X 0 .010 mg/1 PAP 10/31/00 1328
X 0. 010 mg/1 PAP 10/31/00 1328
X 0 .010 mg/1 PAP 10/31/00 1328
X o . 010 mg/1 PAP 10/31/00 1328
X 0.010 mg/1 PAP 10/31/00 1328
0 . 020 mg/1 PAP 10/31/00 1328
X o. 020 mg/1 PAP 10/31/00 1328
X 0 .010 mg/1 PAP 10/31/00 1328
o. 020 mg/1 PAP 10/31/00 1328
0. 010 mg/1 PAP 10/31/00 1328
X 0 .010 mg/1 PAP 10/31/00 1328
X 0. 010 mg/1 PAP 10/31/00 1328
X 0. 020 mg/1 PAP 10/31/00 1328
X 0.010 mg/1 PAP 10/31/00 1328
X o. 010 "'.J/1 PAP 10/31/00 1328
0 .010 mg/1 PAP 10/31/00 1328
X 0 .020 mg/1 PAP 10/31/00 132B
X 0 .010 mg/1 PAP 10/31/00 1328
X o. 020 mg/1 PAP 10/31/00 1328
X 0 .010 mg/1 PAP 10/31/00 1328
X o. 010 mg/1 PAP 10/31/00 1328
X 0. 010 mg/1 PAP 10/31/00 1328
X 0 .010 mg/1 PAP 10/31/00 1328
X o. 010 mg/1 PAP 10/31/00 1328
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 l 816 E. Durst Avenue 1 Greenwood, SC 29649 I [phone] 1 Fax {864) 229-71 l 9
4
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Df\VIS
FLtJfD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA, LLC
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITCI
Parameter
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
wet Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
Result
< 0 .010
o. 010
< 0 .010
< 0 .010
< 0 .010
< 0 .010
< o. 020
0 . 020
< o. 010
1020
Project Number: 61195.00-0004
Report Date November 2 8 , 2000
Page 2 of 2
Sample ID L00102603-02
Qual RDL Units Analyst Date Time
X 0 .010 mg/1 PAP 10/31/00 1328
X 0 .010 mg/1 PAP 10/31/00 1328
X 0 .010 mg/1 PAP 10/31/ 00 1328
X 0 .010 mg/1 PAP 10/31/00 1328
X 0 .010 mg/1 PAP 10/31/00 1328
X o. 010 mg/1 PAP 10/31/00 1328
X 0 . 020 mg/1 PAP 10/31/00 1328
X 0 .020 mg/1 PAP 10/31/00 1328
X 0.010 mg/1 PAP 10/31/00 1328
10.0 mg/1 TRB 11/02/00 1445
I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax {864) 229•71 19
5
DAYIS
FLMD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA, LLC
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID; K-28
Parameter
Field Data
EPA 170.l
TEMPERATURE
SW846 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Wet Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
GW/Chemw
Result
18.0
6.1
777
785.50
163
Project Number, 61195.00-0004
Report Date January 16, 2001
Page 1 of 1
Sample ID L00102603-03
Date Collected: 25-0CT-00 13 :50
Date Received 25-0CT-00
Qual RDL Units Analyst Date Time
1.0 degrees C 10/25/00 1350
0.50 SU 10/25/00 1350
1.0 umhos/cm 10/25/00 1350
. 01 feet MSL 10/25/00 1350
1.0 mg/1. TRB 11/02/00 1530
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue
6
I G,eenwood, SC 29649 I [phone] I Fax [phone] I
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Dl\YIS
FLtwD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA, LLC
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ~-28 DtrP.
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Wet Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
GW/ChemW
Result
18.0
6. l
778
785.50
204
Project Number, 61195.00-0004
Report Date
Page 1 of 1
Sample ID
January 16, 2001
L00102603-04
Date Collected: 25-0CT-OO 13:50
Date Received 25-0CT-00
Qual RDL Units Analyst Date Time
1.0 degrees C 10/25/00 1350
0.50 SU 10/25/00 1350
1.0 umhos/cm 10/25/00 1350
.01 feet MSL 10/25/00 1350
2.0 mg/1 TRB 11/02/00 1551
I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax {864) 229-7119
7
DAYIS
FLtfYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA, LLC
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: V-23
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 90408
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Wet Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
GW/ChemW
Result
l9 .0 .. ,
5060
794.55
10800
Project Number: 61195.00-0004
Report Date
Page 1 of 1
Sample ID
: November 28, 2000
L0010260J-05
Date Collected: 25-OCT-00 14:18
Date Received 25-0CT-00
Qual RDL Units Analyst Date Time
1.0 degrees C 10/25/00 1418
a.so SU 10/25/00 1418
1.0 umhos/cm 10/25/00 1418
.01 feet MSL 10/25/00 1418
100 mg/1 TRB 11/02/00 1615
Davis & Floyd, Inc. \ PO Drawer 428 I Greenwood, SC 29646 I 81 6 E. Durst Avenue l Greenwood, SC 29649 \ [phone] l Fax [phone] l 9
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Df\YIS
FLOYD
Client
Contact
LABORATORY ANALYSIS REPORT
TICONA, LLC Project Number: 61195.00-0004
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Report
Page 1
Date November 28,
of 1
2000
Client ID: TRIP BLANK Sample ID L00102603-06
Matrix
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
l, 1, 2 -TRICHLOROETIW·JB
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE {TOTAL)
GW/ChemW
Result
< 0 .0050
< 0. 0050
< 0 .0050
< 0 .0050
< 0 . 0050
< 0 .0050
< 0 .0050
0.057
o. 010
< 0.0050
0.033
< 0. 0050
< 0 .0050
< 0 .0050
< 0.010
0 . 0050
< o. 0050
< o. 0050
< 0.010
0.0050
< 0.010
< 0 . 0050
< 0 .0050
< 0. 0050
< 0.0050
< 0. 0050
< 0. 0050
< 0. 0050
< 0 . 0050
< 0. 0050
< 0. 0050
0 . 0050
< 0 .010
< 0 .010
< 0.0050
Date Collected: 24-0CT-OO 21: 50
Date Received 25-0CT-00
Qual RDL Units Analyst Date Time
o. 0050 mg/1 PAP 10/31/00 1016
0 . 0050 mg/1 PAP 10/31/00 1016
0.0050 mg/1 PAP 10/31/00 1016
0 . 0050 mg/1 PAP 10/31/00 1016
0 .0050 mg/1 PAP 10/31/00 1016
o. 0050 mg/1 PAP 10/31/00 1016
0 . 0050 mg/1 PAP 10/31/00 l 016
0 .010 mg/1 PAP 10/31/00 1016
0 .010 mg/1 PAP 10/31/00 1016
0.0050 mg/1 PAP 10/31/00 1016
0.010 mg/1 PAP 10/31/00 1016
0.0050 mg/1 PAP 10/31/00 1016
0 . 0050 mg/1 PAP 10/31/00 1016
0 .0050 mg/1 PAP 10/31/00 1016
0.010 mg/1 PAP 10/31/00 1016
0.0050 mg/1 PAP 10/31/00 1016
0.0050 mg/1 PAP 10/31/00 1016
0.0050 mg/1 PAP 10/31/00 1016
0.010 mg/1 PAP 10/31/00 1016
0.0050 mg/1 PAP 10/31/00 1016
0.010 mg/1 PAP 10/31/00 1016
o . 0050 mg/1 PAP 10/31/00 1016
0 . 0050 mg/1 PAP 10/31/00 1016
o.ooso mg/1 PAP 10/31/00 1016
0 .0050 mg/1 PAP 10/31/00 1016
o. 0050 mg/1 PAP 10/31/00 1016
0.0050 mg/1 PAP 10/31/00 1016
0.0050 mg/1 PAP 10/31/00 1016
o.ooso mg/1 PAP 10/31/00 1016
0 . 0050 mg/1 PAP 10/31/00 1016
0. 0050 mg/1 PAP 10/31/00 1016
0 . 0050 mg/1 PAP 10/31/00 1016
0.010 mg/1 PAP 10/31/00 1016
0.010 mg/1 PAP 10/31/00 1016
0.0050 mg/1 PAP 10/31/00 1016
I Davis & Floyd, Inc. I PO Drawer 428 1 Greenwood, SC 29646 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone] l9
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Df\YIS
FLffi'D LABORATORY ANALYSIS REPORT
Master Tracking List
Sample ID
L00102603-0l
Field Data
EPA 170.l
SW846 9040B
SW846 9050
Client
Contact
Gas Chromatography
SW846 8015
Volatile Organics
SW846 8260B
Wot Chemistry
SW846 9060
L00102603-02
l"ield Data
EPA 170. l
SW846 9040B
SWB46 9050
Gas Chromatography
SW846 8015
Volatile Organics
SW846 8260B
Wot Chemistry
SW846 9060
Field Data
EPA 170.1
SW846 9040B
SW846 9050
Wot Chemistry
SWB46 9060
TICONA, LLC
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID
ITEl"
ITCI
K-28
Project Number: 61195.00·0004
Report Date
Page 1 of 2
November 28, 2000
Date Collected
25-0CT-00 12:56
25-0CT-OO 13:08
25-0CT-00 13:50
Date Received
25-0CT-00
10/25/00 1256
10/2s/oo 1256
10/25/00 1256
10/31/00 2240
10/31/00 1303
11/02/00 1428
25-0CT-00
10/25/00 1308
10/25/00 1308
10/25/00 1308
11/01/00 1740
10/31/00 1328
11/02/00 1445
25-0CT-00
10/25/00 1350
10/25/00 1350
10/25/00 1350
11/02/00 1530
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue l Greenwood, SC 29649 I {864) 229-441 3 1 Fax {864) 229-7119
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Sample ID
L00l0260J-04
Field Data
EPA 170.l
SW846 904GB
SWB46 9050
Wet Chemistry
SW846 9060
L00102603-05
Field Data
EPA 170.1
SW846 9040B
SW846 9050
Wet Chemistry
SWB46 9060
L00102603-06
Master Tracking List
Client
Contact
TICONA, LLC
PO BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID
K-28 DUP.
V-23
TRIP BLANK
Volatile Organics
SW846 8260B
Project Number: 61195.00-0004
Report Date November 28, 2000
Page 2 of 2
Date Collected Date Received
25-0CT-00 13:50 25-0CT-00
10/25/00 1350
10/25/00 1350
10/25/00 1350
11/02/00 1551
25-0CT-00 H:18 25-0CT-OO
10/25/00 1418
10/25/00 1418
10/25/00 1418
11/02/00 1615
2'-0CT-00 21150 25-0CT-OO
10/31/00 1016
I Davis & Floyd, Inc I PO Drawer 428 I Greenwood, SC 29648 l 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
11
DAYIS
FLt1YD LABORATORY ANALYSIS REPORT
Method Conformance Summary
Client: Ticona, LLC
Login(s): L00102603
Critetria Volatiles
Sample Holding Time
Standards Preparation
Instrument Tuning
Instrument Calibration
Calibration Verification
Degradation Check
Interference
Sample/Standard
Blanks Results
Method Accuracy
Method Precision
Surrogate Recovery
PDS/SD/MSA
TCLP Preparation
Key ✓
N/A
= Met Criteria Met
= Not Applicable
,J
,J
,J
,J
,J
NIA
N/A
✓
✓
✓
•
N/A
N/A
Semi
Volatiles
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
NIA
N/A
N/A
N/A
N/A
Metals
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
*
PDS =
SD =
MSA=
Method Criteria Not Met -Seefootnote(s) below.
Post Digestion Spike
Serial Dilution
Method of Standard Additions
Project Number: 61995.00-0004
Report Date: November 28, 2000
Inorganics Other
,J ✓
,J ,J
N/A N/A
,J ,J
✓ ,J
N/A N/A
N/A N/A
✓ ✓
✓ ✓
✓ ✓
N/A NIA
NIA N/A
N/A N/A
Footnotes: TOC analyses summarized under column headed "Inorganics".
Ethylene glycol summarized under column headed "Other".
Volatiles -Acetone and 2-butanone were detected in the trip blank. These targets
were also present in sample LOO I 02603-02 (sample ITCI).
Volatiles-The surrogate, 1,2-dichloroethene, recovered high in the MS (124.4%).
The upper control range is 122%. The MSD and LCS yielded similar results
(120.8% and 121.4% respectively) but fell within the range.
Volatiles -The units for the MS/MSD Report and the LCS Report are in ug/L instead
ofmg/L.
Prepared gslwµ
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Davis & Floyd, Inc. I PO D,awe, 428 I G,eenwood, SC 29648 I 816 E. ~u;" Avenue I G,eenwood, SC 29649 I (8641 229-4413 I fax [phone] I
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Df\YIS
FLlWD LABORATORY ANALYSIS REPORT
Surrogates % Recovery
L00102603-0l 31-0CT-00 13 :03
L00102603-02 31-0CT-00 13 : 28
LQ0102603-06 31-OCT-00 10: 16
LCS23705:l 31-0CT-OO 18: 12
MB23705:l 31-OCT-00 09: 03
MS0010251 l -01 :23705 31-0CT-00 11 : 27
MSD00102511-01:23705 31-OCT-00 11 :51
DCE 1,2-DICHLOROETHANE-D4
BFB BROMOFLUOROBENZENE
TOL TOLUENE-DB
113. 4 104. 0
112 .9 103 .6
108 . 3 103. 0
121. 4 103. 8
94.6 102. 2
124. 4 105. 5
120.8 103.6
Report Date
Page 1 of 1
Matrix
Method
96. 3
95.7
96.5
95.0
99. 5
93 . 3
94 .9
November 15, 2000
GW/ChemW
SW846 8260
I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (8641 229-4413 I Fax [phone] l 9
13
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Di\YIS
FLtJ\'D LABORATORY ANALYSIS REPORT I
Method Blanks
Blank : MB23705: l
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETI-W-lE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXAN0NE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHAf.1E
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Cone
' 0.0010
< 0 .0010
< 0. 0010
< 0 .0010
< o. 0010
< 0 .0010
< 0 .0010
' o. 0050
' 0 .0050
< 0 .0050
< o. 0050
< 0 .0010
< o. 0010
< 0. 0010
< 0 .0010
< 0 . 0010
< 0. 0010
< 0. 0010
< 0 .0010
< 0 .0010
< 0 . 0010
< 0. 0010
< 0 .0010
< 0 .0010
< o. 0010
< 0 .0010
< 0 . 0010
< 0 . 0010
< o. 0010
< 0 .0010
< 0 . 0010
< 0 .0010
< 0 .0010
< o. 0010
< 0 .0010
Davis & Floyd, Inc. I PO Drawer 426 I Greenwood, SC 29646 I 816 E. Durst Avenue
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Report Date November 27, 2000
Page 1 of 1
Matrix GW/ChemW
I
WorkGroup: WG23705
Qual RDL Units Analyst Date Time
0 .0010 mg/1 PAP 10/31/00 0903
0. 0010 mg/1 PAP 10/31/00 0903
0. 0010 mg/1 PAP 10/31/00 0903
0 .0010 mg/1 PAP 10/31/00 0903
0 .0010 mg/1 PAP 10/31/00 0903 I
0. 0010 mg/1 PAP 10/31/00 0903
0 . 0010 mg/1 PAP 10/31/00 0903
o. 0050 mg/1 PAP 10/31/00 0903 I
o. 0050 mg/1 PAP 10/31/00 0903
0 .0050 mg/1 PAP 10/31/00 0903
0. 0050 mg/1 PAP 10/31/00 0903
o. 0010 mg/1 PAP 10/31/00 0903 I
0 .0010 mg/1 PAP 10/31/00 0903
0. 0010 mg/1 PAP 10/31/00 0903
o. 0010 mg/1 PAP 10/31/00 0903
0 .0010 mg/1 PAP 10/31/00 0903 I
0.0010 mg/1 PAP 10/31/00 0903
o. 0010 mg/1 PAP 10/31/00 0903
o. 0010 mg/1 PAP 10/31/00 0903 I
0 . 0010 mg/1 PAP 10/31/00 0903
o. 0010 mg/1 PAP 10/31/00 0903
o. 0010 mg/1 PAP 10/31/00 0903
0 .0010 mg/1 PAP 10/31/00 0903 I
0.0010 mg/1 PAP 10/31/00 0903
0.0010 mg/1 PAP 10/31/00 0903
0.0010 mg/1 PAP 10/31/00 0903
0 . 0010 mg/1 PAP 10/31/00 0903 I
0 . 0010 mg/1 PAP 10/31/00 0903
0 .0010 mg/1 PAP 10/31/00 0903
0 .0010 mg/1 PAP 10/31/00 0903 I
0 .0010 mg/1 PAP 10/31/00 0903
0 .0010 mg/1 PAP 10/31/00 0903
0. 0010 mg/1 PAP 10/31/00 0903
0 .0010 mg/1 PAP 10/31/00 0903 I
0.0010 mg/1 PAP 10/31/00 0903
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Df\YIS
FLtfYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
MS00102511-01:23705
MSD00102Sll-01:23705
50.00
50.00
50.00
50.00
50.00
50.00
50. 00
50.00
50.00
50.00
< 5 .00
< 5. 00
< 5 .00
< 5 00
< 5 . 00
MSD
so. 86
52 . 68
51. 36
48. 70
52 .47
Report Date
Page 1 of 1
November 15, 2000
Matrix GW/ChemW
WorkGroup: WG23705
Method SW846 8260B
51. 71
52.39
51. 39
47.94
52. 62
101. 7
105.4
102.7
97.4
104.9
103.4
104 . 8
102. 8
95.9
105.2
.66
0.552
0.0584
.57
0. 285
74-130
89-120
89-115
86-120
86-122
9
10
6
7
12
74-130
89-120
89-115
86 120
86-122
NOTE: MS/MSD % recoveries are not evaluated if the sample concentration is greater than four times the spike added.
I Davis & Floyd, Inc. I PO Drawer 428 \ Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] 1 Fax [phone]
1 5
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Df\YIS
FLtwD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
LCS23705:l
20 00
20 00
20 00
20 00
20 00
20 36
21. 17
20 69
19 40
20 91
Report Date
Page 1 of 1
November 15, 2000
Matrix Gw/Chemw
WorkGroup, WG23705
Method SW846 8260B
101. 8
105.9
103.5
97.0
104 . 6
74-125
90 119
89-116
87-120
86-120
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D1\YIS
FL(jyD
Method Blanks
Blank
Parameter
Gas Chrolll&tography
SW84.6 8015
ETHYLENE GLYCOL
: MB23710:l
LABORATORY ANALYSIS REPORT
Cone
< 7.0
Report Date
Page 1 of 1
November 15, 2000
Matrix GW/Chemw
WorkGroup, WG23710
Qual RDL Units Analyst Date Time
7.0 mg/1 JMT 11/01/00 0213
I Dav;s & Floyd, Inc. I PO Dcawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I fax [phone]
1 7
Df\VIS
FLtn'D LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
ETHYLENE GLYCOL
ETHYLENE GLYCOL
MS00102509-0l:23710
MSD00102509-0l:23710
50.00
50.00
< 7.00
51.06
Report Date
Page 1 of l
: November 15, 2000
Matrix GW/ChemW
WorkGroup: WG23710
Method SW846 8015
55. 78 111. 6 73-116
102. 1 8.85 20 73-116
NOTE: MS/MSD % recoveries are not evaluated i[ the sample concentration is greater than four times the spike added.
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 L Durst Avenue Greenwood, SC 29649 I [phone] I Fax [phone]
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Df\VIS
FLt1YD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS : LCS23710: 1
ETHYLENE GLYCOL 50.00 51.68
Report Date
Page 1 of 1
November 15, 2000
Matrix GW/ChemW
WorkGroup: WG23710
Method SW846 8015
103.4 64-117
I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone] l 9
1 9
DAYIS
FLOYD
Method Blanks
Parameter
Wet Chemistry
SW846 9060
Blank
ORGANIC CARBON, TOTAL
MB23766: 1
LABORATORY ANALYSIS REPORT
Report Date November 15, 2000
Page l of l
Matrix GW/ChemW
WorkGroup: WG23766
Cone Qual RDL Units Analyst Date Time
< 1.0 1.0 mg/1 TRB 11/02/00 1718
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]l l9
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
ORGANIC CARBON, TOTAL
ORGANIC CARBON, TOTAL
MS0010260l-06:23766
MSD00102601-06:23766
20.00
20. 00
20 .23
39. 40
Report Date
Page 1 of 1
November 15, 2000
Matrix GW/ChemW
WorkGroup, WG23766
Method SW846 9060
36.40 80.9 77-121
95.9 7.92 17 77-121
NOTE: MS/MSD \ recoveries are not evaluated if the sample concentration is greater than four times the spike added.
I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (8641 229-441 J I Fax [phone] l 9
21
DAYIS
FLtfYD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS LCS23766:l
ORGANIC CARBON, TOTAL 10.00 9.70
Report Date
Page 1 of 1
: November 15, 2000
Matrix : GW/ChemW
WorkGroup, WG23766
Method : SWB46 9060
97.0 90-110
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. ;~st Avenue I Greenwood, SC 29649 I (864) 229-441 l I Fax [phone] l 9 I
Chain of Custody Record Page_/_ofj_
Client Project I Site Location 816 E. Durst Avenue, Greenwood, SC 29649 [phone] Fax: [phone]ee use urnv
C.N.A. Holding, Inc. 61195.00 LaboratOI}' Certifcation Numbers: SC-24110, NC-25, TN-2923, VA· 77
Shelby,NC Well Samolina
Cootad Report To Copy To Reporting Requirements: { J Standard { ] Data Pack.age (Specify Level) Purchase Order
Johnnv Ledford
CollededBy
Required Parameters, Containers and Preservatives State Quote
'-' ~ a. NC E E ~ E E ~
I
N 0 0 ~ Special Instructions
John McMahan -'-' ~ N L.O~ln
NOTICE: . ~ a
~ 0. ~ ~
:a; .. E ~ g ~
' " 0 • " g' • 8 in € >-. ~ .
:g_ -g ~ ,.,~
• _.g 0 0 C '>
E -~ w 8 -••
:); a; 8. 8. a N ~ ... ~i "'-D . , D • a. ~ • a.
E ~ 8 E iii E 0 0 ,. <J> i~
Samole Collection 0 e , 8 ~ in I. -' i:: .5 .!=.. 0 '-' " z a.
Samr1le Descrintion Date Time Time Tvoe Total B C A A Fraction HOT ommems
Trio Blank 10/24/00 z, .:-a X £' z z. O&
ITEF 10/25/00 I 2 -;'(a X 5 7 I cl ;, I () I
ITCI 10/25/00 1,, s )(' 5 ·7 I 3 2 I 0~
K-28 10/25/00 ,i 3_;,-,::;, ): 5 2 I I 0$
K-28 Due. 10/25/00 /:J':,·-o y 5 ?-I I 04-
V-23 10/25/00 1</16' ;< 5 2., I I 05
-/
R;~~~'.7, Dale Time Re/iquished By Date Time Reliqulshed By Date Time Quick~ Shipp(i;!J·
J(),,Z5't?t> l~lt? y N '"""
/
,---
Received By Dale Time Received By Date Time Recj();.,t•;,:°':J:>/J J / 5 Date Time JI Y, specify: Airbill Number
tO.'/..P.ot /~Jo ,/ days
1 ........ ments Cooler ID ~tie): _.,.,..
On Ice: Ye o Temp(C) 'I-
Custodv Seal: Intact I Broken / 'one
Matrix Type Definitions 1 -Dnnkmg Water 2-Clean Water 5-Groundwater 7 -Soi11Sed1ment 8-Liquid Sludge 9 • Oil 12 • Air Davis & Floyd, Inc.
Preservative Definitions A -Nooe B -H2S04 C -Ha D • HN03 E -NaOH F • mered G -Other
FL02 _ 01 (021'99) -----------------
CNGIHECRS ARCHIT£CTS FIELD DATA LOG
I Df\VIS
FLffi!D Pl.AHH(RS SCCCHHStS
CHARLESTON • C_REENWOOO • COLUMBIA
FOR GROUNDWATER SAMPLE COLLEC,:ION/ I
GROUNDWATER ELEVATION MEASUREMENTS
Well No • ..TTc J;,_
Cfient: /' J/.d_ -Jl,:,Ji.dQ ~• Z:,t. ~
./
Site Nome:Sbe//,7, /.,/C Job No_;,,( //(75.,-1
Dote: ,{_,Q_ -.?:_!2._-.. 0D LWR submilled by: l{,f./-£<,r:c
Sampling Personnel: JLI']
Site Personnel: ✓<!r,,,..,l· M 'H,,._,r,.~ I
Regulatory Personnel: -
Weather Conditions: tfot"£td2 f ,
Temp.: 7b 5
Well Oiameier: z. ,,., In.
(A} Top of Well Devotion: ,,.., cA::.
7
ms! (yes/no)
(B} Depth lo Immiscible Loyer: -rt.
(C} Immiscible Layer [lcvolion: (A)-(B)= -msl (yes/ no)
(0) Depth to Groundwater: N/4 ft.
7
(E) Groundwater Elevation: (A)-(0)= msl (yes/no)
(f) Total Well Depth = ft.
(G) Lenglh of Waler Column: (f)-(0)= ft.
Cosing Volume = (G) x Volume in gol./ft.= \!,I gals.
'FJ,-4 !(/4 Storl Time: Method of Well Evacuation -
Method of Sample ·collection fJ,-4 l, Time: I jOJS
Chain-of-Custody Form Storied ®/no)
-..
Source(s) of Well ID M,a,,,
I 10 label @'no)
Well Complelion: Protective Casing (§/no) nush (yes(®
nush-Mounl Cover Seal Intact (yes(§) Locking Cop (yes~
Locked at Arrival (yes/no) Oeporlure (yes/no) ,,.<f/4
Well Cosing ~ight ob~/depth below) ground: ,,,/4 Cosing Type (PVC) (Steel) (Other)
; /1//,4 Oedicale~ or Hatler (yes/no) Type ,
Protective Post/ Abutment (yes/no} Concrele Pod !:f!j/no)
Well Integrity Solisfoclory {yes/no) If no, exp~low.
Well Yield ( tow / moderate / high }-fr ~
WELL VOLUME DATA
DIA. or PIPE (in.) VOLUME IN GAL/fl.
1.0 0.041
2.0 0.163
3.0 0.367
~-0 0.653
5.0 .. 1.020
6.0 1.470
TO CONVERT GAl/fT TO UTERS/fT, MULTIPLY ABOVE flGURES _BY
3.8 LITERS/GALLON.
fl
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FIELD ANALYSES I 1st Volume 2nd Volume 3rd Volume ~th Volume 6th Volume
Volume Purged (gallons) -
Time (military) I ' "' "'° I pH (S.U.) >-z
Sp. Cond. (umhos/cm) Ii; -Ut
Water Temp. (•c) Zr
Odor (subjective)• -I
Turbidity (subjective),. -
• (!)Hone (2)Slighl (3}Moderole (4)Stronge I " (l)Cleor (2)Slighlly Turbid {3)Moderolely Turbid ( 4)Very Turbid (5)Exlremely Turbid
Commenls/Observafl~ns/Rccommendol1ons: ------------------------------
----------------•
FORM COMPLETE~L2»ft'.~:itA
(SOU.n.ttl)
, lo -z.r-P0
01,: r form48 (3/94) I
24 I
I
..• DFLJ\YIDS [HGIHC[RS ARCHITECTS Lm.r PL4HN(RS SO(NTISIS
FIELD DA TA LOG
FOR GROUNDWATER SAMPLE COLLEC110N/
GROUNDWATER ELEVATION MEASUREMENTS
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CHARU:STOH • C.REEHWOOD • COLUMBIA Well No · IT J:: /' . ..
Client: f" J/.d-J/,z.f.i.do.,f,, 'L,t_ ~ Source(s) of Well ID Maa ID Label @lno)
., I
Site Hame:Sbe/671 /JC Job Ho.:/ 1105.. I Well Completion: Proleclive Cosing @/no) Rush (yes@
.
Cale: L_2_-.ZS'.--oo LWR submilled by:/,{,/,,/_ /4,-r nush-Mounl Cover Seal tnlacl (yes.(§} Locking Cop (yes~
Sampling Personnel: J Lh -Locked at Arrival (yes/no) Departure (yes/no) •/4
Well Casing (E"ight ab~/deplh below) ground: //. ~
Sile Personnel: Jer,-\: f/<-Hu_.cce-y "
7 /J /A.
Regulatory Personnel: -Casing Type {PVC) (Slee!) (Other)
Wealher Conditions:t/vc: /,: a :1 /
I Dedicate~ or Bailer (yes/no) Type /ft'/4
Temp.: :Ze f /
Well Oiameler: z_ ,,., In. Protective Post/ Abutment (yes/ no) Concrete Pad @/no)
(A) Top of Well £1evalion: /v' / ,' ms! (yes/no) Well Integrity Salislactory (yes/no) It no, explain below.
,
( law / moderate / high )-r1/4
(B) Oep!h ta Immiscible Layer: -ft. Well Yield
(C) Immiscible Layer [levalian: (A)-(B)= ..... ms! {yes/no)
(0) Depth to Groundwater. ft. WELL VOLUME CATA
(E) Groundwater Elevation: (A)-(0)= ms! (yes/no)
OIA. Of PIPE (in.) VOLUME IH GAL/fl.
1.0 0.041
(f) Total Well Oepth = ft. 2.0 0.163
3.0 0.367
(G) Lenglh of Water Column: (F)-(0)= , ft. 4.0 0.653
Casing Volume = (G) x Volume in gat./ft.= ,V
5.0 .. 1.020
gals. 6.0 1.470
.
Method of Well Evacuation 'i5,, I!:! 1 p N/4 Start Time: ,-TO COHVERT GAL/FT TO UT£RS/FT. MULTIPLY ABOVE RGURES BY
Method of Sample "Collection p . Jc Time: I z '[6
3.8 UT£RS/GALLOH.
bc..?IU> I
Chain-al-Custody form Started {@/no)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged {galloni) -
Time (mffilory) I z ::re
pH (S.U.) 5,z
Sp. Cond. (umhos/ cm) ? z.c, ,?
Water Temp. (•c) z. '
Odor {subjoctive)• -
Turbidity (subjective)" -
• (l)Hone {2)Slight (3)Moderale (4)Stronge
" (1)Ctear (2)Slightly Turbid (3)Moderolely Turbid (4)Very Turb[d (5)Extremely Turbid
Comments/Observafi?ns/Recommendalions: ------------------------------
,Oo, ro_.ITT~~
0 ,LQ=.ij-.c>C> .
o&: r Form48 {3/94)
25
CHCIHCCRS ARCHITECTS
I
FIELD DATA LOG D1\YIS
FLffi!D PlANH(RS SCCCHTISTS
CHARU:STOH • G,REEHWOOD • COLUMBIA
FOR GROUNDWATER SAMPLE COLLECTION/ k 8 I
GROUNDWATER ELEVATION MEASUREMENTS -;i. ])4.J) Cf'-
. · Well No · t!C Z g
er.en!: /" J/J._. J/,11/4L-t1q_.f.,,I-'1."-
Site Home: 5:belby, ,1-,(c Job Ho.:t.:'.' /lc?.5., /
Dote: /P -~ S, ,c,c, LWR submilled by: ,s'.'£0,t:J, -,f"v-18
Sampling Personnel: JLt:J -
Sile Personnel; J ... ,,'7 M1 t':1"-v:r::•y
Regulatory Pmonnel: -
Weather Conditions:&, u,x:c,...._sf I Temp.: 7D S
Well Oiomeier. z,,.,-, In.
(A) Top of Well Elevation: f>/1,20 msl (yes/no)
(B) Depth to Immiscible Loyer. -It.
(CJ Immiscible I.ayer [levalion: (A)-(B)= -msl (yes/no)
(D) Depth lo Groundwater. z s; za ft.
{E) Groundwater Elevation: (A)-(D)= 7 S 5". '>-q-msl (yes/no)
(F) Total Well Depth = .i28'.oo ft.
(G) Length of Woler Column; (F)-(D)= 2-3 ft.
Casing Volume = (G) x Volume in gat./ft.= (!). 1:. gals.
Method of Well Evacuation pl.,..l:!:l p. Starl Time: / ?3,:
Method of Sample 'Collection ?'-<-at I) lime:/ 357;>
J
Chain-of-Custody form Storied ®/no)
. ..
Source(s) of Well ID M.:aa I ID label (§Yno)
Well Complelion: Protective Cosing @/no) flush (yes@
nush-tJounl Cover Seal Intact {yes{§) Locking Cop (yes~
Lacked al Arrivol~no) Deporlure l.iJ/no)
Well Cosing (!ieighl obo~/deplh below) ground; 4cJ
Cosing Type (PVC)~ (Other)
Dedicate~ or Boiler (yes/no) Type
Proleelive Post/ Abutment I({,)/ no) Concrete Pod @/no)
Well Integrity Satisfactory ~no) If no, explain below.
Well Yield ( tow / moderate /~
WELL VOLUME DATA
DIA. or PIP[ (In.) VOLUME IN GAL/Fl.
1.0 0.041
2.0 0.163
3.0 0.367
4.0 0.653
5.0 " 1.020
6.0 1.470
TO CONVERT GAL/FT TO UTERS/FT. MULTIPLY ABOVE llGURES BY
3.8 UTERS/GALLON.
fl.
"
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FIELD ANALYSES Pcy?
1St Volume 2nd Volume 3rd Votumo -4th YelYmO 6th Volume
Volume Purged (gallon~) t,. </ A .c, J. 4'
Time (military) /-:.: _.,/,,.., I z,,, I J ",I<( I pH (S.U.) L ,.-1 l-. I ,:._ I C. I
Sp. Cand. (umhos/cm) .<,:u:, "1 lf'O "1-, .., 7 9
Water Temp. (•c) lo I~ I -? /,s I Odor (subjective)• z. z 'Z-
Turbidity (subjective)" 2-2 z. -
• (t)None (2)Slighl (3)Moderale (4)Slronge I " (l)cteor (2)Slighlly Turbid (3)~oderolety Turbid (4)Very Turbid (S)Extremely Turbid
Comments/Observati~ns/Recommendalions: ------------------------------
----------------1
""'~~,~1' (~II.ft)
OAT . /o-.? >--:.,po
O& r form48 (3/94) ,I
26 I
I
I DFLt'WIDS EHGIH[[RS ARCHITECTS Lffi.r Pt.ANtC(RS SO(HHSJS
FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLl;C"flON/
GROUNDWATER ELEVATION MEASUREMENTS
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CHARU:STON • G.REENWOOD • COLUMBIA Well No· V-2 5 ..
Cfienl: CJ/1-Jblc/u':fS,,Me. Source(s) of Well ID M,," ID label (§Yno)
I
S~e Hame:Sbelby, /JC Job Ho.:/ l!Cl5.o ' Well Completion: ProlecHve Casing ~no) flush (res@
Dale: I/J-z.-,: _. ,DC, LWR submil!ed by: J{,1842,. -f!/,tR nush-Mount Cover Seal Intact (yes@ Locking Cop (yes@l
Sampling Personnel: JLh lacked al Arrival ~/no) Deparlur..-@/no)
Site Personnel: J,-,,-rt tJ. r M4J. cc~{ Well. Casing ~ighl aboJt/dcplh below) ground: 3.D ti,
Regulatory Per..onnel: Casing Type (PVC)~ (Other)
Weather Conditions: @<'. r C<L s ,f---I Temp.: 70 .S Dedicate~ or Bailer (yes/ no) Type
Well Oiameler: z.~ In. Proleclive Posl/Abulmenl (yes/!!§) Concrete Pad @/no)
(A) Top of Well [levalion: >f u. 'fi':i msl (yes/no) Well lnlegrily Solisfaclory liJi/no) II no, explain below.
(B) Depth lo Immiscible Layer. -fl. Well Yield ( low / moderate /@
(C) Immiscible Layer [levalion: (A)-(B)= -msl (yes/ no)
(0) Depth lo Groundwater: , ,.~4 fl. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(0)= 7 '7~ J:;'msl (yes/no)
DIA. OF PIPE (in.) VOLUME IH GAL/Fl.
1.0 0.041
(F) Talol Well Oeplh = ,z ,3, ,) fl. 2.0 0.163
3.0 0.367
(G) Length al Waler Column: (F)-(0)= ~.oc fl. 4.0 0.653
5.0 .. 1.020
Casing Volume = (G) x Volume in gal./fl.= t_.v gals. 6.0 1.470 -
Method of Well Evacuolion R..;n f? Slarl Time: 1 <I S7 TO CONVERT GAL/FT TO UTERS/FT, MULTIPLY ABOVE flGURES BY
' 3.8 UTERS/GALLON.
Method of Sample Collection ?L<-mD Time: Iii 1?
I
Chain-of-Custody Form S!arled ®/no)
flELO ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged (gallon~) Iv z. 0 3. <>
Time (military) /,(J/Pt? I 4.,,, ~ I <f/ ,{
pH (S.U.) i/. !? '-). q ,c,,4
Sp. Cond. (umhos/cm) Si q cJ s-,oo '.">-.-~L ..-.
Waler Temp. (•c) i tf I Cf' , a
Odor {subjective)• 3 ;i :,
Turbidity (subjective)" 2-;, L
• {!)None (2)Slighl (3)Moderole (4)Stronge
" (1)Ctear (2)Slightly Turbid (3)Yoderalely Turbid (4)Very Turbid (5)Exlremely Turbid
Comments/Observations/Recommendations: ------------------------------
o& r form48 (3/94)
27
Kubal-Furr & Associates
-E11viro11111t:11lal Co11s11ltn11ts-
Dote: ________ _
Personnel: ________ _
Well ID MPE {II msl) Depth lo
Water (II)
A-39 823.36 ;};;). , l '-"
B-34 790.62 ('3.73
C-49 864.11 0--d-. '1 'B
D-27 845.50 ;:}. I , q 'S"
D-35 845.69 :);,-."IS
D-56 845.19 o-1 .9 3
D-88 845.52 d-a-. d-0
F-55 849.19 3<i,dt
G-50 848.48 3Co-io9
G-88 848.26 3 ~.<S'G
H-59 845.25 43.53
H-79 846.23 4<..,,. ?It
t-57 837.63 Y?:,. -:,o
J-29 825.18 J.'o ''-<'9
J-59 825.01 J\.,,,l\l
K-28 811.20 ';)<=;'. 70
K-58 81 1.39 ';}~ 'J..:>
M-28 806.72 3\.o<:,
M-44 806.71 '30,'9<.o
N-29 803.38 \B.~7
N-53 803.82 IC\ , o \
0-25 807.54 [l,.(o(,
0-59 806.61 /S'.39
P-31 790.00 d4-,,C11
P-58 788.12 8-d-. '2, lo
0-33 783.48 d'S°, (.,,3
R-17 779.31 /d-,((,,
R-42 778.81 11.os-
S-50 826.02 3,l,.J-1,.
T-17 777.90 13. t:>
T-35 777.38 l;},efC
T-58 776.03 s.~
\do S:-f'
CNA Holdings, Inc. -Shelby, North Corolino
Water-Level Measurements
Page: ___ __ct_o:,,;1_4 ___ _
Meter: ________ _
Comments Well ID as it Appears on
Well
' I \ \..1-.J'-"-. ~ ~ I a..&:e ~f:iid E:F,;:0 "i'$
28
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Kubal-Furr & Associates
-E11virn11me11f11l Cons11ltn11ts-
Date: ________ _
Personnel: ________ _
Well ID MPE (ft msll Depth lo
Waler (fl)
U-38 826.55 "30. II,,
V-23 811.89 /7,34-
W-23 800.91 \,. 0·7
X-32 796.96 /<..,. =
Y-38 794.52 ctd--\\
Y-74 794.87 19 .o.::.
Z-78 797.08 o, :,.00
AA-41 783.68 :,'c, '\ C
AA-54 782.16 ::,~.7"1
BB-18 771.75 l'.l,B5
CC-33 812.68 ;) t, . I ;:;,
CC-64 811.37 cl-.... , l., 3
DD-58 796.10 ~S-~
EE-58 794.48 ·:is .63
FF-23 772.33 I ~ .e::D
FF-34 772.73 ):).a-7
FF-62 772.19 1 3."'i'l
GG-25 771.64 d-1-ss
GG-39 770.44 <'}o .,5(
GG-61 771.78 0-\.~C)
HH-48 755.44 4-~Sl)
HH-77 755.87 4<)..S7
PZ-1 773.99 l't':..a-\
PZ-2 795.81 ?J7.70
CNA Holdings, Inc. -Shelby, North Carolina
Water-Leve! Measurements
Page: ___ ...:2'-"o'--f _:.4 __ _
Meter: ________ _
Comments Well ID as it Appears on
Well
PZ-3 Wei/ Destroyed/Paved Over in Late 1995
PZ-4 750.07 IN\\!\
PZ-5A 788.72 '34,<;3
PZ-5B 777.59 eA-. ~ti
PZ-6A 795.1 I ?,:')_ i<o
PZ-6B 796.89 :5\,,,8)
PZ-7A 780.46 ~'\. 55
PZ-7B 784.46 v• '1 \,
29
Kubal-Furr & Associates
-E1wiro11111e11tal Co11sulta11ts-
Date: ________ _
Personnel: ________ _
Well ID MPE (II msl) Depth to
Waler (11)
PZ-8 767.99 4_9c;
PZ-9 788.96 "2>/t.£l\
PZ-10 784.65 ?,"l. 3 <,,
PZ-11 805.48 ss.c0
PZ-12 749.41 "BO->-'<"'"
PZ-13 776.51 N ""-
OT-IR 771.44 N 't"'-
OT-2R 773.55 s:?A
OT-3 792.88 ;;,.S.S\o
OT-4 790.28 ~;)..'$ \
OT-5 784.00 ,}3.11<;'
OT-6 787.45 o3 ."\7
OT-6A 798.68 ~ C:-.'33
OT-7 782.16 '::,d-.cl \
OT-7A 782.52 "1 .o<j
OT-8 782.26 IL.43
OT-10 804.08 >s.13
IT-I 814.20 w \I\
IT-2 813.85 N Iv'-
IT-3 809.66 NI"
IT-4 809.08 ::, ;).. Cf 0
IT-5 810.64 ~ ,_,,_, I/
IT-6 812.20 73-S-flil
IT-7 813.52 "?J-1.~
IT-8R 813.04 &4-:;Sl
IT-9 808.73 \;J tJ\
PEW-I 846.85 4lt ."I (
34.70
CNA Holdings. Inc. -Shelby, North Carolina
Water•Level Measurements
Page: ___ --'3'--"a'-1 ~•---
Meter: ________ _
Comments Well ID as it Appears on
Well
PEW-2 Well Abandoned in Lale 1996
PEW-3 849.25 '3'6.dl.Cl
PEW-4 848.14 3--S-S7
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Kubal-Furr & Associates
-E11vironme11tal Co11s11ltants-
Dale: ________ _
Personnel: ________ _
Well ID MPE (It msl) Depth lo
Waler (fl)
TD-\ 17. 4-:;-
TD-2 6\c-6\o
TD-3 ::; 'a.I :,
TD-4 -4 0, <.o'l
T-1 \\.. l (I,\
T-2 f--..)""
Tl-\ ~ l S::>
Tl-2 ?:,l,~J
S-1 .'.27,9"1
31
CNA Holdings, Inc. -Shelby, North Carolina
Water-Level Measurements
Page: ____ 4'-"-ofc...c4 __ _
Meter: ________ _
Comments Well ID OS ii Appears on
Well
DAVIS & FLOYD, INC.
LOGIN REPORT (ln0l)
October 26 2000, 08:04 am
Login Number: L00102603
Account: HNAHOL-SHE TICONA,LLC
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Project: 61195.00-0004 GW S&A (REPLACES 60885.00-0004) I
!liiiill!\ll~ml IIii!l!l !llm§§;r l liillcer•· I II'.iiill(4
•·· ill iili i <
LQ0:tCJ26 .. 03S0]. ITE:f \2.5:'QCTS2.0.00 \12 :5§ 25-'.OCT-'2000> S PH · ············ Remarks
GW/Chemw
GW/Chemw
GW/ChemW
GW/Chemw
GW/Chemw
GW/ChemW
GW/Chemw
S FL/GWE/MSL
S FL/PH
S FL/SPCO
S FL/TEMP/C
S WC/TOC
S VO/8260/TCL
S GC/EG
*0
*0
*0
*0
REF-0 *l
REF-4 *2
REF-0 *3
NA
)•···~~::~~;~::,
I
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••··· <•••••·•?••••·•2·.5+QC'\f/i:2o·.bb •••••tJ ,·b9•••••••2•·5••;ocT·"2•b··oo•>s t··•·.q:zf.N9YP•2p•q•·I ··· ············ ptt·······.•.•.• ...... Remarks
GW/ChemW
GW/ChemW
GW/ChemW
GW/Chemw
GW/Chemw
GW/Chemw
GW/ChemW
S FL/GWE/MSL
S FL/PH
S FL/SPCO
S FL/TEMP/C
S WC/TOC
S VO/8260/TCL
S GC/EG
*0
*0
*0
*0
REF-0 *l
REF-4 *2
REF-0 *3
,.y ,I I
I
L0 .. bl.02··6•0·35.03/• /Kf2.•9·•••·•·••··nr···•·• ····•·•···•·••.•• t••·Ittt•·•>•·••·••·•••·•••t?••••2·5·£OcT.·f2·•0•.ob• •••I3•,s•i~•2•·5•FoQ[!~~•~·~;s <···•.07f.NOY.+2·oql
GW/ChemW S FL/GWE/MSL *0 !YA
GW/ChemW S FL/PH *0
GW/ChemW S FL/SPCO *0
GW/Chemw s FL/TEMP/C *0 I
GW/Chemw S WC/TOC REF-0 *l
··/25SOC'Tf:2b0Q \l.3i5g~25f()Cit~~~~;;s•• to7fNQy~2 001 ·
S FL/GWE/MSL
S FL/PH
S FL/SPCO
*0
*0
*0
*0
tyJ I GW/ChemW
GW/Chemw
GW/ChemW
GW/ChemW
GW/ChemW
S FL/TEMP/C
S WC/TOC REF-0 *l
· · · \25b.09'.!'E2•oo•q 14 :}8\25S99Tf2·000\$ Y o7\N9Yt2.ool
GW/Chemw
GW/ChemW
S FL/GWE/MSL
S FL/PH
COC Record rese ent)
*0
*0
Sample Conditwn Intact Broken!Leakin~)
Info on COC Recor: sand Samples Agree Ye /No)
Sample Temp. I/. Received on Ice Ye No)
Work request (Presenttif!senJf>
Quote Number n'A
Page 1
32
PH Remarks
;/.,A
.L
Reviewed:
Signature:
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DAVIS & FLOYD, INC.
LOGIN REPORT (lnOl)
October 26 2000, 08:04 am
Login Number: L00102603
Account: HNAHOL-SHE TICONA,LLC I Project: 61195.00-0004 GW S&A (REPLACES 60885.00-0004)
n···15···············t· ··········•···············•········ cmruent .•.•···•·.··.··. ncommect• ........ ·ttecieliN'etn ........ · ·nue
GW/ChemW S FL/SPCO *O J:)
r/ChemW S FL/TEMP/C *O ±
1w/ChemW S WC/TOC REF-0 *1
1·001Q26Q3HoEi. /rRTP>B4ANK/••·•·•--··· · · ·.·· ?2<1+ocrt2000/ 21/50 2?SQc:Tq2ooor s•· ?/rJ7\NQY.+2•000
PH Remarks
W/ChemW S V0/8260/TCL REF-4 *1 NA
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Page 2
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~~~ LABORATORY ANALYSIS REPORT
Explanation of Symbols and Abbreviations
The following defines common symbols and abbreviations used in reporting technical data:
RDL Report Detection Limit MDL Method Detection Limit
TOP Top of Pipe MSL Mean Sea Level
TNTC Too Numerous To Count MPN Most Probable Number
BTU British Thermal Units NTU Nephelometric Turbidity Units
C Degrees Centigrade F Degrees Fahrenheit
umhos/cm micromhos/cm meq milliequivalents
kg kilogram(s) g gram(s)
mg milligram(s) ug microgram(s)
I liter(s) ml milliliters(s)
ul microliter(s) m3 cubic meter(s)
lb pound(s) ft3 cubic foot(feet)
ft foot(feet) TIC Tentatively Identified Compounds
mg/I, mg/kg Units of concentration in milligrams per liter for liquids and milligrams per kilogram for solids. Also
referred to as Parts Per Million or "ppm" when the assumption is made that the specific gravity or
density is one (1 g/ml).
ug/I, ug/kg Units of concentration in micrograms per liter for liquids and micrograms per kilograms for solids.
Also referred to as Parts Per Billion or "ppb" when the assumption is made that the specific gravity
or density is one (1 g/ml).
wt¾ Units of concentration expressed on a weighUweight basis (e.g. grams per 100 grams).
< Less Than -The number following the sign is the limit of quantitation, the smallest amount of
analyte that can be reliably determined using this test.
> Greater Than
Data Qualifiers:
A
B
C
E
J
p
X
•
TIC is a possible aldol-condensation product resulting from sample extraction, (Organics)
Analyte also detected in the method blank.
Amendable Cyanide is a negative value due to an unknown interference.
Estimated concentration due to interference.
Estimated value below RDL or estimated value for TIC. (Organics)
Concentration difference between primary and confirmation columns >25%. (Organics) The lower result is
reported.
Matrix interference which requires dilution or prevents the reporting of a result. Detection limits have been
adjusted where applicable.
Defined in report comments .
Solid samples (i.e. soil, sludge, and solid waste) are reported on a dry weight basis unless othenwise noted.
Test results relate only to the sample tested. Clients should be aware that a critical step in a chemical or biological
analysis is the collection of the sample. Unless the sample analyzed is truly representative of the bulk of the material
involved, the test results will be meaningless. If you have any questions regarding the proper techniques of collecting
samples, please contact us. However, we cannot be held responsible for sample integrity unless sampling has been
performed by a member of our staff.
WARRANTY AND LIMITATION OF LIABILITY -The accuracy of all analytical results is warranted for the sample as
it is received by the laboratory. Warranty for the integrity of the sample begins at the time it is placed in the
possession of authorized Davis & Floyd, Inc. Laboratories personnel. All other warranties, expressed or implied, are
disclaimed. Liability is limited to the cost of the analysis.
Davis & Floyd, Inc.
AD07_0/ (07/99)
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Davis & rloyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649
34
I [phone] I fax (8f,4) 229-71191
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I Attachment 3
I Selected Water-Quality Plots
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Kubal-Furr & Associates
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-------------------
4000 ~------
3500 · · · · · · · · · · · · · · ·
3000 · · · · · · · · · ·
~ 2500
E ~
C 0 :;:: 2000 ., ... -C Cl)
() 5 1500 u
1 000 ·
500 · · · · · ·
Inner Tier Combined Influent TOC Data
ITCI TOC Data
o~.----+-----+-------+----+-------t-----+-----+------+-~
1/1/93 1/1/94 1/1/95 1/1/96 12/31/96 12/31/97 12/31/98 12/31/99 12/30/00
Date
-------------------
ITCI Ethylene Glycol Data
Location Date Value Unit
ITCI 11/29/94 2330 mg/L J ITCI Ethylene Glycol Data
3/7/95 1800 mg/L 4000 -
5/1 8/95 1000 mg/L JL
8/22/95 209 mg/L 3500 ------

-

-
---

-
11 /29/95 52 mg/L z
11 00 mg/L :J' 3000 -----

-
-

-
-
1/16/96 -4/ 1 5/96 1 070 mg/L D>
.S 2500 --

-

-
--

-

-

-

-

-

-

-
-
7/12/96 550 mg/L C:
10/31/96 840 mg/L 0 16 2000 ----

-
---

-

-
-
1/17/97 603 mg/L ~ -C:
4/29/97 1560 mg/L ~ 1500 -
7 /22/97 1430 mg/L C: 0
1 0/28/97 111 0 mg/L U 1000 ---
1 /22/98 99 mg/L 500 -
5/7/98 1310 mg/L
7/21/98 596 mg/L 0 -
1 0/20/98 550 mg/L 11/29/ 11 /29/ 11/28/ 11/28/ 11/28/ 11/28/ 11/27 /
1/14/99 665 mg/L 94 95 96 97 98 99 00
4/8/99 1510 mg/L
8/19/99 310 mg/L Date
11 /9/99 1040 mg/L
02/08/00 1440 mg/L
4/27/00 3760 mg/L
7/19/00 802 mg/L J
10/25/00 779 mg/L
-------------------
V-23 TOC Data
14000 -.------------------------------------7
12000 · · ·
1 0000 ·
:J' -Cl
.§.. 8000
C: 0 ;::; .. ~ -a; 6000 ·
(,)
C: 0 u
4000 ·
2000 ·
o -L. -----+-----+------+--~~_J~--------1
-
2
-
1
--1
2
,....9-
19
-s--1-2-12-+9-1:---9-a-~1~2-::12::8100
1/1/85 1/1/87 12/31/88 12/31/90 12/30/92 12/30/94
Date
-------------------
Monitor Well V-23 2-Butanone Data (MEK)
Location Date Value Unit
V-23 8/3/89 1 . 1 mg/L V-23 2-Butanone (MEK)
11 /9/89 0.45 mg/L
1/5/90 0.37 mg/L
2/23/90 0.038 mg/L 4 -
8/8/90 0.56 mg/L
11/7/90 0.01 mg/L u 3.5
2/5/91 0.66 mg/L
mg/L 3 ---

-

-
-

-
5/3/91 0.46 -..J u u -i C
8/9/91 0.04 mg/L Cl C '" .S 2.5 --

-

-
&l --

-

-
-

-

-

-
0:, -

-

-
------
mg/L u :;; => 11/4/91 0.05 N 0
C 0 :l
2/4/92 0.2 mg/L 0
-i_
0 ., 2 --:1 ::_ -: _ 1 _: --5/5/92 0.2 mg/L u "' ~ -8/7/92 0.8 mg/L C ~ 1.5 -
11 /6/92 0.1 mg/L u C 0
2/3/93 0.05 mg/L u (.) 1 -
5/5/93 0.25 mg/L u
8/6/93 0.044 mg/L 0.5 -
11 /3/93 0.01 mg/L u
2/2/94 0.25 mg/L u 0 -
8/5/94 0.52 mg/L 6/1 /89 6/1/91 5/31/93 5/31/95 5/30/97 5/30/99
3/8/95 0.01 mg/L < Date
8/24/95 0.767 mg/L >
1/16/96 3.6 mg/L
7/12/96 0.5 mg/L
1/17/97 0.591 mg/L
7 /22/97 0.01 mg/L <
1/22/98 0.164 mg/L
7/21/98 0.466 mg/L
1/14/99 0.34 mg/L
7/21/99 0.27 mg/L J
2/8/00 0.19 mg/L
7/19/00 0.42 mg/L
-------------------
Location
V-23
Date
8/3/89
11 /9/89
1 /5/90
2/23/90
8/8/90
11/7/90
2/5/91
5/3/91
8/9/91
11/4/91
2/4/92
5/5/92
8/7/92
11 /6/92
2/3/93
5/5/93
8/6/93
11 /3/93
2/2/94
8/5/94
3/8/95
8/24/95
1/16/96
7/11/96
1/17/97
7 /2 2/97
1 /22/98
7/21/98
1/14/99
7/21/99
2/8/00
7/19/00
Value
0.1
0.295
0.3
0.34
0.31
0.01
0.52
0.53
0.48
0.53
0.08
0.2
1 . 1
0.14
0.05
1
0.025
0.01
0.36
0.52
0.01
0.648
0.487
1 . 15
0.818
0.05
0.01
1 .22
0.005
0.27
0.22
0.47
Unit
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/I
mg/I
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
u
u
B
u
E
u
B
u
J
<
<
J
<
J
Monitor Well V-23 Acetone Data
----------------------------.
V-23 Acetone Data
1.4 -~-------------------7
1 .2 ·
;!' 1 en .§.
c: 0 8 · 0 .
:;:: ..
!:: 0 6 · C: . ..
" 5 0.4 ·
0
0 -~. -~>-t--_.:._~.___,~----+-v--o~e---
6/1 /89 6/ 1 /91 5/31 /93 5/31 /95 5/30/97 5/30/99
Date
-------------------
Monitor Well V-23 Benzene Data
Locatign Date Value Unit
V-23 8/3/89 0.05 mg/L u
11 /9/89 0.005 mg/L u
1 /5/90 0.019 mg/L J
2/23/90 0.031 mg/L V-23 Benzene Data
8/8/90 0.02 mg/L u
11/7/90 0.013 mg/L 0.3 -
2/5/91 0.022 mg/L J
5/3/91 0.013 mg/L J
8/9/91 0.04 mg/L u 0.25 --

-

-
-

-

-
. ---

-
-
11/4/91 0.015 mg/L J ::::;-
2/4/92 0.012 mg/L J ci 0.2 · -~ . -~ C s "' 5/5/92 0.071 mg/L J Ji 00 " N 00 :', =>
8/7 /92 0.05 mg/L u C 0
0 ; 0
11 /6/92 0.017 mg/L J ~ 0.15 I l l ~
mg/L J -2/3/93 0.006 C
Cl)
5/5/93 0.25 mg/L u u 0.1 C
mg/L J 0 8/6/93 0.004 u
11 /3/93 0.022 mg/L 0.05 -

-
-. -. ----
2/2/94 0.25 mg/L u
8/5/94 0.022 mg/L J
3/8/95 0.011 mg/L < 0 -
8/24/95 0.0293 mg/L 6/1 /89 6/ 1 /91 5/31 /93 5/31/95 5/30/97 5/30/99
1/16/96 0.0193 mg/L Sample Date
7/11/96 0.0291 mg/L ----~ -----------------------------------
1/17/97 0.01 78 mg/L
7 /22/97 0.02 mg/L
1/22/98 0.0104 mg/L
7/21/98 0.0207 mg/L
1/14/99 0.014 mg/L
7/21/99 0.018 mg/L
2/8/00 0.012 mg/L
7/19/00 0.021 mg/L
- - - - - - - - - - -·--

-

-

-

-

-

-
K-28 TOC Data
9000·.---------------------------------------7
8000 ·
7000 ·
~ 6000 · · · ·
.J -Cl
E
; 5000 ·
0 = "' .. c: 4000 ·
Cl> u
C 0
U 3000 ·
2000 ·
1000 ·
o~liJ.--+---+----+---+-------==--::~~_-=:::::,.1-o-<_.__..r.hti1a---1..._.w=..J
9/1/81 9/1/83 8/31/85 8/31/87 8/30/89 8/30/91 8/29/93 8/29/95 8/28/97 8/28/99
Date
-------------... -----Monitor Well K-28 Benzene Data
Location Date Value Unit
K-28 8/4/89 0.022 mg/L
11/9/89 0.005 mg/L u
1 /4/90 0.015 mg/L K-28 Benzene Data
2/ 19/90 0.025 mg/L u
5/4/90 0.018 mg/L
8/8/90 0.03 mg/L 0.035 ~ t C
mg/L g w
11 /6/90 0.015 "' N :,
2/6/91 0.019 mg/L :; 0
0.03 o·
5/3/91 0.014 mg/L J
. -l -8/8/91 0.017 mg/L l 11/4/91 0.03 mg/L J -0.025 ·
.J
2/4/92 0.017 mg/L C)
5/5/92 0.017 mg/L J .s 0.02
0.019 mg/L C: 8/7/92 0 .:
11 /6/92 0.009 mg/L J .. ~
2/3/93 0.009 mg/L J i: 0.015 .,
0.014 mg/L u 5/5/93 C: ---l--mg/L 0
8/6/93 0.015 u 0.01 -
11 /3/93 0.011 mg/L
2/2/94 0.014 mg/L • in
0.018 mg/L 0.005 -N
8/8/94 :,
3/9/95 0.006 mg/L 0
8/23/95 0.0205 mg/L 0 '
1/16/96 0.0086 mg/L 6/1 /89 6/ 1 /91 5/31 /93 5/31 /95 5/30/97 5/30/99
7/11/96 0.0149 mg/L
1/17/97 0.005 mg/L <
Date
7 /22/97 0.01 mg/L
1 /22/98 0.007 mg/L
7/21/98 0.0126 mg/L
1/14/99 0.01 mg/L
7/21/99 0.01 mg/L
2/8/00 0.0092 mg/L
7/19/00 0.01 mg/L
-------------------
HH-48 TCE Data
Location Date Value Unit
HH-48 8/3/89 0.16 mg/L
11/7/89 0.14 mg/L
2/5/90 0.005 mg/L u
5/1 /90 0.17 mg/L
8/2/90 0.15 mg/L HH-48 TCE Data
11 /2/90 0.15 mg/L
2/1/91 0.15 mg/L
5/2/91 0.12 mg/L 0.25 -
8/2/91 0.01 mg/L u
11/1/91 0.16 mg/L
2/3/92 0.16 mg/L 0.2 -- -- ----- - --
4/30/92 0.15 mg/L
8/3/92 0.18 mg/L ::r 11/3/92 0.22 mg/L E "' 2/1/93 0.15 mg/L .§.0.15-- --------
5/3/93 0.18 mg/L C: 0
8/2/93 0.2 mg/L :;::: .. ~
11/1/93 0.22 mg/L E -C: ., 0.1 -- ------ - -
1/31/94 0.2 mg/L u
C:
8/1 /94 0.16 mg/L 0 u
8/1/94 0.01 mg/L
3/8/95 0.17 mg/L 0.05 -- ------
8/23/95 0.222 mg/L
1/17/96 0.165 mg/L
7/12/96 0.179 mg/L
1/17/97 0.15 mg/L 0 -.
7/22/97 0.09 mg/L 6/30/89 6/30/91 6/29/93 6/29/95 6/28/97 6/28/99
1 /22/98 0.101 mg/L Date
7/21/98 0.08 mg/L
1/14/99 0.088 mg/L
7/21/99 0.084 mg/L
2/8/00 0.09 mg/L
7/19/00 0.072 mg/L
-------------------
HH-77 TCE Data
Location Date Value Unit
HH-77 TCE Data
HH-77 8/3/89 0.008 mg/L
8/2/90 0.04 mg/L 0.45
8/2/91 0.13 mg/L 0.4 -
8/3/92 0.067 mg/L '.J" 0.35 ---

-

-
--

-
--

-
--

-
--

-
8/2/93 0.12 mg/L "c;
8/1 /94 0.12 mg/L s 0.3 -. -

-
-
8/23/95 0.332 mg/L 5 0.25 -
1/17/96 0.187 mg/L -.;:. .. 0.2 --

-
-

-

-

-
---~
7/12/96 0.383 mg/L -C
1/17/97 0.224 mg/L 1l 0.15 ----------
C
7 /22/97 0.26 mg/L 0
(.) 0.1
1 /22/98 0.0754 mg/L
7/21/98 0.225 mg/L 0.05
1/14/99 0.13 mg/L 0
7/21/99 0.25 mg/L 6/ 1 /89 6/1/91 5/31 /93 5/31/95 5/30/97 5/30/99
2/8/00 0.078 mg/L Date
7/19/00 0.14 mg/L