NCD003446721_20010312_Celeanse Corporation - Shelby Fiber_FRBCERCLA SAP QAPP_New (North) Tank Farm Area Soils Assessment-OCR

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Post Office Box 2732 I 0
Tampa, FL 33688-3210
[phone]
FAX [phone]
k fatpa@cart h Ii n k .net
Mr. Jerry McMurray
Ticona ES&H, Shelby Plant
Post Office Box 87
Shelby, NC 28150
Kubal-Furr & Associates
Enviro11me1Ital Consultants
March 12, 200 I
Re: New (North) Tank Farm Area Soils Assessment
Kubal-Furr Project No. TF026Ml01
Dear Mr. McMurray:
Post Office Box 80247
Simpsonville, SC 29680-0247
[phone]
FAX [phone]
[e-mail]
SUPERFUNO SECTION
. Kubal-Furr & Associates is pleased to submit this letter report summarizing the work
performed and laboratory analyses related to the soil samples collected at the new tank farm area.
These samples were collected by Kubal-Furr on March 1, 2001.
Work Performed
The site proposed for the new tank farm is an undeveloped strip of land approximately 120 x 40
ft localed adjacent to and just north of the existing north tank farm (Figures 1, 2). In January of
200 I, Law Engineering drilled a series of geotechnical borings at the site and reported "chemical"
odors in the shallow soil samples. In response to the Law Engineering report, Ticona retained
Kubal-Furr lo conduct additional investigations of the area and lo collect depth-discrete soil
samples for laboratory analysis of selected site-related constituents.
At each of five soil boring locations sited by Ticona, Kubal-Furr hand-augered and collected
five grab soil samples for soil vapor screening and laboratory analyses. Samples were collected
directly from the auger bucket with a stainless-steel spoon. Each sample set consisted of one 4-
ounce and one 8-ouncc sample collected in unpreserved glass jars, and three 40 mL VOA vials
preserved with sodium bisulfate. A portion of each sample (approximately 4 ounces) was also
placed into a zip-lock bag for soil vapor screening in the field. A clean (field decontaminated) auger
bucket was used for each sample, and all sampling equipment was cleaned between boreholes.
Soil vapors were measured by inserting the probe of a Photovac 2020 Photoionization meter
(PIO) into the zip-lock bag and directly reading the maximum concentration on the LED read-out.
Soil vapor measurement ranged from a low of 16.6 ppm lo several samples reported at >2000 ppm.
Table I is a summary of the field soil vapor screening results.
Of the 25 samples collected and screened in the field, eight were selected for further laboratory
analyses. The samples selected for laboratory analysis were generally the samples showing the
highest PIO readings and included NTF0l-2 (boring #1, depth 2 ft bis), NTF0l-13, NTF02-7,
NTF02-I 4, NTF03-5, NTF03-13, NTF04-13 and NTF05-8. The samples were shipped via FedEx
to Shealy Environmental Services of Cayce, South Carolina. Laboratory analysis consisted of
volatile organic compounds (VOCs) by EPA Method 82608; semivolatile organic compounds
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Mr. Jerry McMurray -2-March 12, 2001
(SVOCs), including 1,1-biphenyl and diphenyl ether by EPA Method 8270C; ethylene glycol,
diethylene glycol, and methanol by EPA Method 8015B; and, acetic acid by EPA Method 300.0.
Discussion of Analytical Findings
The highest concentrations of constituents reported by the laboratory correlated well with the
field soil vapor screening results. A summary of the analytical results and constituents detected are
presented in Table 2. A copy of the laboratory data report, data quality assessment and field
sampling logs are included in Attachment 1.
Acetone, ethylene glycol, MEK, and acetic acid were the principal constituents reported in the
13-14 ft depth samples from boreholes NTF0l, NTF02, and NTF03, and the 5-ft sample from
NTF03. In addition, phenol was reported as present in both the 5-ft and 13-ft samples from
borehole NTF03. Only low levels of acetone and methylene chloride were reported in the shallow
samples from borings NTF0I, NTF02, the 13-ft sample from boring NTF04, and the 8-ft depth
sample from NTF05. Based on these data, the highest concentrations and most frequent detection
of constituents occurred adjacent to the existing North Tank Farm and the northern horizontal
extent of contamination appears limited principally to an area within 25-ft of the retaining wall.
In addition to the analytical results, Table 2 presents selected NCDENR or EPA soil action
criteria for the reported constituents. These criteria were obtained from the following sources:
•
•
•
•
Table 4.1: Soil Remediation Goals (RG's) contained in the NCDENR's Inactive
Hazardous Sites Program (IHSP) "Guidelines for Assessment and Cleanup" (August
2000).
Table 3: Contaminated Soil Clean-Up Levels (soil-to-groundwater) in the NCDENR's
"Groundwater Section Guidelines for the Investigation and Remediation of Soil and
Groundwater" (July 2000).
Absent remediation levels in either of the above documents for the reported constituents, the
USEPA Region IX Preliminary Remediation Goals (October 1999) were substituted.
Further, Kubal-Furr also relied on the NCDENR document entitled: "Remediation Process
Plan-2000" for additional guidance in evaluating the data.
Based on these guidelines, none of the constituents reported as present exceeded either the
IHSP RG's or the Region IX PRGs. The only constituent reported to exceed a DENR clean-up
level was acetone, which exceeded the Groundwater Section level of 2.81 mg/kg in three samples at
two locations: NTF-02-14 (8.5 mg/kg), NTF-03-05 (5.3 mg/kg) and NTF-03-13 (4.0 mg/kg).
No free product or any evidence of a "fresh" or on-going releases were found during the
boring program. During the test borings, it was noted that the materials sampled in the upper 10-14
ft consisted of fill material and that native soils were not encountered until about 13-14 ft bis. From
a geologic standpoint, it appears that the acetone and other constituents have migrated downward
through fill and encountered the lower permeability native soils which may have retarded further
vertical migration. This would explain the highest concentration of constituents typically found at
depth rather than in the shallower soils.
Kubal-Furr & Associates
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Mr. Jerry McMurray -3-March 12, 2001
Comparison of Findings to Other Site Data
Acetone is a constituent that has been reported as present in ground-water, soil and sediment
samples collected at the site going back to the original remedial investigations. During the RI, it was
one of the most frequently reported constituents, being present in 62 ground-water samples at an
arithmetic mean concentration of 0.41 mg/L, and in 12 surface soil samples (including the area of
the North Tank Farm) at a mean concentration of 0.305 mg/kg. It was also reported as present in 8
off-site ground-water samples at a mean concentration of 0.040 mg/L. In the risk assessment
conducted during the feasibility study, acetone was not selected as an indicator chemical" ... due to
its low toxic potential. Acetone is naturally present in human blood and urine as a by-product of
metabolism (Verschueren, 1983)."
Review of the Shelby database (1989 to present) indicates acetone reported as present in 173
samples, 81 of which are ground-water samples. Of the 81 ground-water results for.acetone, only 7
were reported to exceed the State's MCL of 0.70mg/L-all at wells K-28 (2 occurrences) and V-23
(5 occurrences). Of the 7 reported exccedences, 4 of the results were qualified in some fashion as
either estimated or present in a blank sample. Therefore, while acetone is frequently reported as
present in ground-water samples, it is generally reported as present at levels below the State MCL.
Closing Comments
In summary, the soil sampling program at the new tank farm area indicated the presence of
selected site-related constituents, only one of which (acetone) exceeded any established guidance
concentration. No free product or any evidence of a "fresh" or on-going release were found during
the boring program. In addition, it appears that the horizontal extent of constituents is principally
limited to the area adjacent to the existing North Tank Farm, near the retaining wall.
Our understanding is that the upper two feet of soil will be excavated and the area backfilled
with a concrete pad to support the new tanks. Regarding further action at the proposed site, we
would recommend that the material removed be stockpiled until composite samples can be collected
to determine disposal options. Based on our test boring program and analysis of the upper soils, it
does not appear that disposal will require a secure landfill. While the deeper soils that remain in
place may have levels of acetone that exceed a soil to ground-water clean-up level, this area will be
capped with a concrete pad which will preclude any direct recharge and further potential for
continuing release to the ground-water system and an alternate concentration level for these soils
appears justified.
Kubal-Furr appreciates the opportunity to have assisted Ticona with this project. Please call if
you have any questions and/or comments regarding this report or if we can be of further assistance.
Sincerely,
Kubal-Furr & Associates
~ t-erry E. Kubal, P.G. ·
C License # 212
Kubal-Furr & Associates
-----
0
0
Legend
0 ,,
♦ ◊ O...otT".,,.E<!r_,_, • + .....,T..,E,ma,o,,w.t -{J--+-P!cWE.onct,o,,w.1
C R-~V .... ■
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""°"""' ..... ,ciu-·-.... ~ • ....,o,.,.,r,..E.,n<tmn,,,_.
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,luo;lPENE,...,._,,.,.. .............. ,_~ .... ,
0-<ISI>•---.,~
- -
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--- ---
Approximate location of New Tank Farm Soils Assessment
Recreation Pond
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80C
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Kubal-Furr & Associates
-Envirorime11tnl Consultm,ts -
Figure 1-Sit-e Location
Cclant:£-e Norch America, Inc.
Shelby. Ncrr.h C,uo/,rt,1
-
I Legend
I • Sample Location
I Railroad Tracks
I Pumps
I • NTF01
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I NTF04 •
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I t: '-.
~
-"' s::
I ~
.s:: 1:: c:, NTF05 • z I ~ C)
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\I) c:,__ • NTF03
I t: ti:'
I 0 5 10
Scale in Feet
2C 30 50 -----
I Kubal-Furr & Associates
-Enviromnenta/ Consulta11ts-
I Figure 2. Sample Location Map
I Project No. -26MI0I
Celanese North America, Inc.
Shelby, North Carolina
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I Table 1. Summary of Soil Vapor Screening
New Tank Farm Soils Assessment
(samples collected 3/1/01)
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Sample ID Time Sampled PID Reading (ppm) I NTF02-2 9:40 513
I NTF02-7 9:50 1535*
NTF02-l 0 10:05 588
NTF02-l 2 10:08 >2000
I NTF02-l4 10:30 >2000*
I NTF0l-2 l l :00 334*
NTF0l-5 l l :l 0 36.3
NTF0l-8 l l :20 113
I NTF0l-l l 11:35 167
NTF0l-13 l l :45 >2000*
I NTF03-2 13:20 183
NTF03-5 13:30 703*
I NTF03-8 13:45 198
NTF03-l l 14:00 143
I NTF03-l 3 14:05 >2000*
NTF04-2 14:35 43.2
I NTF04-5 14:45 42
NTF04-8 14:55 37.9
NTF04-l l 15:05 16.7 I NTF04-l 3 15:10 31.2*
I NTF05-2 15:40 34.8
NTF05-5 15:50 21.5
NTF05-8 16:10 42.7*
I NTF05-l l 16:15 19.8
NTF05-l3 16:20 16.6
I * Samples chosen for further laboratory analyses
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-- - -- -
GW Section
Parameter IHSP RG's Clean-up Levels
Acetone 1560 2.81
Acetic Acid NE11 l'E
Ethylene Glycol 100,00021 l'E
MEl{ 9400 0.69
Methylene
Chloride 85 0.02
Phenol 9400 l'E
1/ NE = not established
2/ AG based on EPA Region IX PRGs
- - ---Table 2. Summary of Analytical Results
New Tank Farm Soils Assessment
-
(all results reported in mg/kg-dry weight)
Samples Collected on March 1, 2001
NTF-01-02 NTF-01-13 NTF-02-7 NTF-02-14
0.043 2.5 0.03 8.5
<0.39 1800 <0.38 700
<64 440 <64 130
<0.016 0.48 <0.015 0.25
<0.008 <0.0079 <0.0074 <0.0078
<0.42 <0.42 <0.42 <0.42
-- -- - --
NTF-03-5 NTF-03-13 NTF-04-13 NTF-05-08
5.3 3.6 <0.031 0.053
1900 1600 <0.4 <0.38
<65 <64 <66 <64 UJ
0.4 0.52 <0.016 <0.014
0.0078 0.0096 0.012 0.0087
1.9 1.5 <0.43 <0.42
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I Attachment 1
I Laboratory Analytical Results, DQA
and Field Sampling Logs
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I Kubal-Furr & Associates
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DATA ASSESSMENT SUMMARY CHECKLIST AND REPORT-LEVEL II
Client ID:
Project Number:
CNA Holdings, Inc.-Shelby
TF026MIOI
Sample Delivery Group (SDG) Description:
Prepared By: Diane M. Rosseter
Date: 3/8/01
Eight soil samples were collected from the new tank farm excavation area at the Ticona/KOSA plant
site by Kubal-Furr and Associates and submitted to Shealy Environmental Services, Inc., of Cayce, SC,
for analysis of volatiles, semi volatiles (including 1, 1-biphenyl and di phenyl ether), ethylene glycol,
diethylcnc glycol, methanol, and acetic acid. Samples were analyzed according to EPA/NCDENR
approved methodology.
CONTENTS LEVEL COMMENTS
JI
Sample Results ..[ All data Class A except as noted in
the discussion section below.
Method Conformance Summary
Chain(s) of Custody (COCs) ..[ Sample collection date missing from
first page; collection time for NTF-
05-8 given as 1610 instead of 1605.
No effect on data.
Master Tracking List ..[ O.K .
Case Narrative ..[ O.K.
Sample Prep
Standards Prep
Instrument Quality Control Data
Batch Quality Control Report ..[ O.K.
Surrogate Recovery Report ..[ O.K.
Trip/Field/Equipment Blank Report ..[ O.K.
Field Notes/Logbook ..[ O.K.
CLP Forms
All Raw Data
Electronic Deliverables ..[ O.K.
Kubal-Furr & Associates
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26MI01-DAS - 2 -3/8/01
Discussion:
1) Ethylene glycol and diethylene glycol recovered below the laboratory established acceptance
limit in the matrix spike performed on NTF-05-08. Results for ethylene glycol and
diethylcne glycol in NTF-05-08 were non-detected, and therefore, flagged with "UJ".
UJ = not detected at the associated sample quantitation limit, however, results should be
considered as estimated
Class A = quantitative Class B = qualitative Class C = unusable
Kubal-Furr & Associates
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SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Kubal-Furr And Associates
PO Box 80247
Simpsonville, SC 29680
Attention : Jim Furr
Project Name: Shelby, NC
Lot Number: CC02001
Date Completed: 03/08/2001
Project Manager
Tctal number of pages in report: 61
This report sh all not be reproduced, except in its entirety, with out the written approva I of Shealy Environmental Services, Inc.
The follo\\ing non-paginated documents arc considered part of this report: Chain Of Custody Record and Sample Receipt Checklist.
111111111111111111111111111111111111111111111 Page I of 61
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SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
Kubal-Furr And Associates
Lot Number: CC02001
This Rcpo,1 of Anal y.;is con ta ins the analytical rcsul t(s) for the samplc(s) listed on the Sample Summary following this page.
Sample ;ma\ ysis ;.rnd data review ha vc been pcrfom1ed in accordance with Shca!y's Quality Assu ranee Management Plan and Standard
Operating Prcx.:cdu res. Any data qualifiers associutcd with SJ rnplc analysis arc footnoted on the analytical rcsu Its pagc(s) or arc discussed
below.
The surrogate recoveries for the volatile dilutions(Run 2)wcrc outside the acceptance criteria for samples CC02001-004 & OOG
<luc to sample matrix. The di.lutions were analy.lcd twice and surrogates failed both times.
The RPO for the SVOC MS/MSD, sample CC02001-00 I, was outside the acceptance criteria.
The RPD and MS/MSD recoveries for ethylene glycol and dicthylcnc glycol were outside the acceptance criteria for sample
CC02001-008.
Upon lab receipt, s:.unplcs were transferred to appropriate sampling containers per prep Method 5035 for VOC analysis.
Page: 2of61
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.Sample Number
I 001
002
003
I 004
005
006
I 007
008
009
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Sample ID
NTF-02-7
NTF-02-14
NTF-01-2
NTF-01-13
NTF-03-5
NTF-03-13
NTF-04-13
NTF-05-8
Trip Blank
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Kubal-Furr And Associates
Lot Number: CC02001
Matrix
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Solid
Aqueous
Date Sampled
03/01/200 I 0950
03/01/2001 1030
03/01/2001 1100
03/01/2001 1145
03/01/200 I 1330
03/01/200 I 1405
03/01/2001 1510
03/01/2001 1610
03/01/2001 0000
Page: 3 of 6 I
I SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
~c DHEC No. 32010 NC DEHNR No. 329
Jtient:
Jttention:
PO Number: 26M101
t escription
ot Number
NTF-02-7
CC02001-00 I
03/02/200 I
Kubal-Furr And Associates
PO Box 80247
Simpsonville, SC 29680
Jim Furr
Project Name: Shelby, NC
Run
I
Analytical Method
82608
Dilution Factor Analysis Date
0J/02/200 I 111 J
larameter
CAS Prep Analytical
Number Method Method
J Volatile Organic Compounds by GC/MS
cetone 67-64-1 5035 8260B
Benzene 71-43-2 5035 8260B
,,omodichloromelhane 75-27-4 5035 8260B
romoform 75-25-2 5035 8260B
Bromomethane {Methyl bromide) 74-83-9 5035 8260B
,-Bulanone (MEK) 78-93-3 5035 8260B
arbon disulfide 75-15-0 5035 8260B
Carbon tetrachloride 56-23-5 5035 8260B
lhlorobenzene 108-90-7 5035 8260B
hloroethane 75-00-3 5035 8260B
Chloroform 67-66-3 5035 8260B
Chloromethane (Methyi chloride) 74-87-3 5035 8260B
tibromochloromethane 124-48-1 5035 8260B
1, 1-Oichloroethane 75-34-3 5035 8260B
1,2-Dichloroethane 107-06-2 5035 8260B 11, 1-Dichloroethene 75-35-4 5035 82608
cis-1,2-0ichloroethene 156-59-2 5035 8260B
trans-1,2-0ichloroethene 156-60-5 5035 8260B
.1.2-0ichloropropane 78-87-5 5035 8260B
cis-1,3-0ichloropropene 10061-01-5 5035 8260B
trans-1,3-0ichloropropene 10061-02-6 5035 8260B
I1,4-0ioxane 123-91-1 5035 8260B
Ethylbenzene 100-41-4 5035 8260B
2-Hexanone 591-78-6 5035 8260B
I4-Methyl-2-pentanone 108-10-1 5035 8260B
Methylene chloride 75-09-2 5035 8260B
Foolnotc(s) @ An:.ilyzcd by Mctrohm-Pcak, Inc.
Date Sampled
Matrix
Percent Solid
03/01/2001 0950
Solid
78.3
Analyst
RED
Prep Date Prep Batch
Result Q PQL Units
30 30 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 15 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 370 ug/kg
ND 7.4 ug/kg
ND 15 ug/kg
ND 15 ug/kg
ND 7.4 ug/kg
PQL = Practical quantitation ltmit B"' Detected in the method blank E = Quantitation of compound exceeded the calibration range
Run
ND= Not detected at or above the PQL J = Estimated result less than the PQL Soils reported on a dry weight basis unless !lagged with a "W"
IS\IEALY E:--:VlROS:-.lENTALSERVJCES, INC.
I0{i Vantage Point Drive, Cayce, SouthCarolimi 29033 [phone] Fax [phone] www.sheal)t:nvironmenta1.com Page: 4 of 61
NTF-02-7
CC02001-00 I
•scription
ot Number
ient
te Received
Kubal-Furr And Associates
03/02/200 I
I
lrameter
Run Analytical Method
82608
I Volatile Organic Compounds by GC/MS
yrene
1, 1,2,2-Tetrachloroethane
l trachloroethene
luene
1, 1, 1-Trich!oroethane
11,2-Trichloroethane
ichloroethene
Vinyl acetate
lnyl chloride
lenes (total)
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I Surrogate
! ,2-Dichloroethanc•d4
Toluenc-d8
Bromofluorobenzene
Runt
Q % Recovery
72
82
78
otnote(s): @ Analyzed by r-.ktrohm-Pcak, Inc.
Dilution Factor
CAS
Number
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
108-05-4
75-01-4
1330-20-7
Acceptance
Limits
70-1 JO
70-1 JO
70-I JO
B = Detcc!L'd in the method blank
Analysis Date
03/02/200 I 1113
Prep Analytical
Method Method
5035 82608
5035 82608
5035 82608
5035 82608
5035 82608
5035 82608
5035 82608
5035 82608
5035 82608
5035 82608
Date Sampled
Matrix
Percent Solid
03/01/2001 0950
Solid
78.3
Analyst
RED
Prep Date Prep Batch
Result Q PQL Units
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 7.4 ug/kg
ND 15 uglkg
ND 7.4 uglkg
PQI. = Practical qu:rntitation limit
ND= Not dctt:cted al or above the PQL J = Estimated result less than the PQL
E = Quantitation or compound exceeded the calibration range
Soils reported on a dry weight basis unless flagged with a "W"
!EALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Driw, Cayce, South Carolina 29033 [phone] Fa.'<. [phone] v.lww.sheal)enVironmental.com Page: 5 of 61
Run
Description NTF-02-7 Date Sampled · 03/01/2001 0950 I Lot Number CC0200I-00 I Matrix Solid
Client Kubal-Furr And Associates Percent Solid 78.3
Date Received 03/02/200 I I
R"n Analytical Method Dilution Factor Analysis Date Analyst Prep Date Prep Batch
8270C 03/03/2001 1155 MWK 03/02/2001 0940 2227 I 2 8270C 0310212001 1723 ~!WK 0J/0212001 0940 2227
CAS Prep Analytical I Parameter Number Method Method Result Q PQL Units Run
Semivolatile Organic Compounds by GC/MS I Acenaphthene 83-32-9 35508 8270C ND 420 uglkg 2
Acenaphthylene 208-96-8 35508 8270C ND 420 ug/kg 2
Anthracene 120-12-7 35508 8270C ND 420 uglkg 2 I Benzo(a}anthracene 56-55-3 35508 8270C ND 420 uglkg 2
Benzo(a}pyrene 50-32-8 35508 8270C ND 420 ug/kg 2
Benzo(b }f!uoranthene 205-99-2 35508 8270G ND 420 uglkg 2 I Benzo(g ,h ,i)perylene 191-24-2 35508 8270C ND 420 ug/kg 2
Benzo(k }fluoran thene 207-08-9 35508 8270C ND 420 uglkg 2
Benzoic acid 65-85-0 35508 8270C ND 11000 ug/kg 2 I Benzyl alcohol 100-51-6 35508 8270C ND 420 ug/kg 2
1, 1-Biphenyl 92-52-4 35508 8270C ND 420 ug/kg
4-Bromophenyl phenyl ether 101-55-3 35508 8270C ND 420 ug/kg 2 I Butyl benzyl phthalate 85-68-7 35508 8270C ND 420 uglkg 2
4-Chloro-3-methyl phenol 59-50-7 35508 8270C ND 420 ug/kg 2
4-Chloroani!ine 106-47-8 35508 8270C ND 420 uglkg 2 I bis(2-Chloroethoxy)methane 111-91-1 35508 8270C ND 420 uglkg 2
bis(2-Chloroethyl )ether 111-44-4 35508 8270C ND 420 ug/kg 2
bis ( 2-C h!oroisop rop yl )ether 108-60-1 35508 8270C ND 420 uglkg 2 I 2-Chloronaphthalene 91-58-7 35508 8270C ND 420 ug/kg 2
2-Chlorophenol 95-57-8 35508 8270C ND 420 uglkg 2
4-Chloropheny! phenyl ether 7005-72-3 35508 8270G ND 420 ug/kg 2 I Chrysene 218-01-9 35508 8270C ND 420 uglkg 2
Di-n-butyl phthalate 84-74-2 35508 8270C ND 420 uglkg 2
Di-n-octylphthalate 117-84-0 35508 8270C ND 420 ug/kg 2 I Dibenzo(a,h)anthracene 53-70-3 35508 8270C ND 420 uglkg 2
Dibenzofuran 132-64-9 35508 8270C ND 420 ug/kg 2
1,2-Dichlorobenzene 95-50-1 35508 8270C ND 420 ug/kg 2 I 1,3-Dichlorobenzene 541-73-1 35508 8270C ND 420 ug/kg 2
1,4-Dichlorobenzene 106-46-7 35508 8270C ND 420 ug/kg 2
3,3'-Dichlorobenzidine 91-94-1 3550B 8270C ND 1100 ug/kg 2
2 ,4-Dichlorophenol 120-83-2 35508 8270C ND 420 ug/kg 2 I Oiethylphthalate 84-66-2 35508 8270C ND 420 ug/kg 2
Dimethyl phthalate 131-11-3 35508 8270C ND 420 ug/kg 2
2.4-Dimethylphenol 105-67-9 35508 8270G ND 420 ug/kg 2 I 4,6-0initro-2-methy\phenol 534-52-1 35508 8270C ND 1100 uglkg 2
2,4-Dinitrophenol 51-28-5 35508 8270G ND 1100 ug/kg 2
2, 4-Dini trotoluene 121-14-2 35508 8270C ND 420 ug/kg 2 I 2,6-0initrotoluene 606-20-2 35508 8270C ND 420 ug/kg 2
Fuul11Lltt:(s) · @Analyzed by Mctrohm-Pcak, Inc. I l'QL = Practical quantitation limit Il .. Detected in the method blank E = Quantitation of compound cxcet:dcd 'the calibration range
ND= Not dt:tccted ut or ubovc the PQL J = Estimated result less than the PQL Soils reported on a dry weight basis unless !lagged with a "W"
Slll.:ALY ENVIRO:--.:~lEt\'TAL SERVICES, INC. I 10() V:111tagc Point Driw, Co.yce, South Carolina 2903] (303) 79!-9700 Fax [phone] V.",','W.shic:31;,\:nvimnmental.com Page : 6 of 61
NTF-02-7
CC0200 I -00 I
•script ion
t Number
Client I tc Recci vcd
Kuba(.furr And Associates
03/02/2001
I
I
Parameter
Run
2
Analytical Method
8270C
8270C
Semivolatile Organic Compounds by GC/MS
Oiphenyl ether
1(2-Elhylhexyl)phthalate
oranthene
Fluorene
lxachlorobenzene
xachlorobutadiene
Hexachlorocyclopentadiene
lxachloroethane
eno(1,2,3-c.d)pyrene
lsophorone
IMethylnaphthalene
Methylphenol
3 & 4-Methylphenol
'Nitrosodi-n-propylamine
Nitrosodiphenylamine
aphthalene
INitroaniline
Nitroaniline
Nitroani!ine
Nitrobenzene
INitrophenol
Nitrophenol
Pentachlorophenol
l•nanlhrene
enol
Pyrene
12,4-Trichlorobenzene
4 ,5-T richlorophenol
2,4,6-Trlchlorophenol
I
Runl
Surrogate Q '¼, Recovery
T erphenyl-d 14 92
Nitrobenzcne-d5 72
I 2-F\uorobiphenyl 90
2-Fluorophenol 72
Pheno!-d5 69
2,4,6-Tribromopheno! 67
otnote(s) @ Analyzed by Metrohm-Peak, Inc.
Dilution Factor
CAS
Number
101-84-8
117-81-7
206-44-0
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
106-44-5
621-64-7
86-30-6
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
87-86-5
85-01-8
108-95-2
129-00-0
120-82-1
95-95-4
88-06-2
Acceptance
Limits
J0-130
]0-130
J0-130
]0-1]0
]0-130
30-IJ0
l'QL = Practical qu;intitation limit B = Detected in the method blank
Analysis Date
0J/OJ/200 I I I 55
0J/02/200 I I 723
Prep Analytical
Me1hod Method
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
Ruu2
% Recovery
80
75
7]
81
77
81
Date Sampled
~fatrix
Percent Solid
03/01120010950
Solid
Analyst
tv!WK
MWK
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Acceptance
Limits
JO-I JO
]0-130
30-1 JO
JO-I JO
]0-130
JO-I JO
78.3
Prep Date
0J/02/200 I 0940
0J/021200 I 0940
Q PQL
420
420
420
420
420
420
1100
420
420
420
420
420
860
420
420
420
420
420
420
420
420
1100
1100
420
420
420
420
420
420
Prep Batch
2227
2227
Units
uglkg
uglkg
uglkg
uglkg
uglkg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
uglkg
uglkg
uglkg
uglkg
ug/kg
ug/kg
E = Quantitation of compound exceeded the calibration rangi:
ND= Not dctecti:d at or abovi: the PC;IL J = Estimated rcsul! less than the PQL Soils reported on a dry weight basis unless flagged with a "W"
IEAI.Y ENVIRONMENTAL SERVICES, INC.
I Ou \';rn1:ige l'uint Oriw, Cayce, South Carolin.:i 290 33 [phone] Fa.-..: (803) 791-911 l W\\W.she-.il)environmenta!.com Page: 7 of 61
Run
1
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
Description
Lot Number
Client
D~Hc Rccci vcd
NTF-02-7
CC0200 I -00 I
Kubal-Furr And Associates
031021200 I
Hu11 Analytical Ml'thod
80158
Dilution Factor Analysis Date
0J/021200 I I 635
Date Sampled
Matrix
Percent Solid
0310112001 0950
Solid
78.3
Analyst
MTR
Prep Date Prep Batch
I
I
I
Parameter
CAS
Number
Prep Analytical
Method Method Result Q PQL Units Run I
GCDAI
Diethylene glycol
Ethylene glycol
Foutnutc(s) @ Analyzed by Metrohm-Peak, Inc.
PQL = Practical quantit:ition limit
ND-Not dctcctcd at or above thc PQL
SHEALY ENVIRON:-..IEi\'T AL $ERV ICES, INC.
111-46-6
107-21-1
B -Detected in the method blank
J = Estimated result less than the PQL
80158
80158
ND
ND
64
64
mg/kg
mg/kg
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight basis unless !lagged with a "\V"
106 Vantage Point Drive, Cayce, South Carolina 29033 (S03) 791-9700 Fax [phone] \\IWV,l,sheal:>environmenta!.com Page: 8 of 61
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·scription
t Number
Client ltc Received
I
IJrameter
l GCDAI
thanol
I
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I
NTF-02-7
CC02001-00 I
Kubal-Furr And Associates
0J/02/2001
Run· Analytical ;\lcthod
8015B
Dilution Factor
CAS
Number
67-56-1
iotnote(s) @ Analyzed by Metrohm-Peak, Inc.
B = D,:tcct<!<l in the method blank
Analysis Date
031051200 I 09 I 5
Prep Analytical
Method Method
80158
Date Sampled
Matrix
Percent Solid
03/01/20010950
Solid
78.3
Analyst Prep Date Prep Batch
MTR
Result Q PQL Units
ND 1.3 mg/kg
Run
l'QL = Practical quantitation limit
ND= Not detected at or above the PQL J = Estimated result less than the PQL
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight b:isis unless flagged with a "W"
!EALY ENVIRm,;~tENT AL SERVICES, li\C.
J U(i Vantage Point DriH:, Cayce, South Carolina 290 33 (S03) 791-9700 Fax (S03) 791-9111 wwv.·.shca!J"'!nVimnmental.com Page: 9 of 61
Description
Lot Number
Client
Date Rcct:ivcd
NTF-02-7
CC02001-00 I
Kubal-Furr And Associates
03/02/200 I
Run Analytical Method
300.0
Dilution Factor Analysis Date
0J/03/2001 0959
Date Sampled 03/01/2001 0950
Matrix Solid I
Percent Solid 78.3
I
Analyst Prep Date Pn·p Batch
@ I
Parameter
CAS
Number
Prep Analytical
Method Method Result Q PQL Units Run I
Subcontracted
Acetic acid
Footnotc(s): @ Analyzed by Mctrohm-Peak, Inc.
PQL = Pr:.H.::tical quantitation limit B = Detected in thi;: metho<l blank
ND .. Not d<:tcctcd at or above the l'()L J = Estimated result !ess than the PQL
SI IEAL Y ENVIRONMENTAL SERVICES, INC.
300.0 ND 0.38 mg/kg
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight-basis unless !lagged with a "W"
l 06 V;intage Point Driw, Cayce, Soulh Carolina 29033 [phone] Fax_ [phone] wv.w.sheal~nvironmental.com Page: 10 of 61
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l scriµtion
t Number
Client ltc· Rcccin:d
I
I
1'.TF-02-14
CC02001-002
Kubal-Furr And Associates
03/02/200 I
Run
2
Analytical Method
82608
82608
Dilution Factor
50
Analysis Date
0)102/2001 1146
03105/200 I 1533
Prep Analytical
Date Sampled
t\fo.trix
Percent Solid
03/01/2001 1030
Solid
77.1
Analyst
RED
RED
Prep Date Prep Batch
Parameter
CAS
Number Method Method Result Q PQL Units Run I Volatile Organic Compounds by GC/MS
Acetone
l nzene
omodichloromelhane
Bromoform
lomomethane (Methyl bromide)
Butanone (MEK)
Carbon disulfide
i3rbon tetrachloride
11!orobenzene
Chloroethane
lloroform
loromethane (Methyl chloride)
bromochloromethane
,
1-0ich!oroethane
2-Dichloroethane
, 1-Dichloroethene
cis-1,2-Dichloroethene
l ns-1,2-0ichloroethene
, 2-Dichloropropane
cis-1,3-Dichloropropene
l ns-1,3-Dichloropropene
,4-0ioxane
Ethylbenzene
IHexanone
Methyl•2•pentanone
Methylene chloride
l yrene
1,2,2-Tetrachloroethane
Tetrachloroethene rluene
1, 1-Trichloroethane
1, 1,2-Trichloroethane
l ichloroethene
nyl acetate
Vinyl chloride
rlenes (lolal)
otnote(s) @ An:ilyzed by Mi.:trohm•Peak, Inc.
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
124-48-1
75.34.3
107-06-2
75.35.4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
123-91-1
100-41-4
591-78-6
108-10-1
75-09-2
100-42-5
79.34.5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
108-05-4
75-01-4
1330-20-7
B = Detected in th..: mdhod blank
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
l'QL = Practical quantitation limit
ND= Not detected at or above the PQL J = Estimated result less than the PQL
!EALY ENVJRON~IENTAL SERVICES, INC.
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
8500
ND
ND
ND
ND
250
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1300
7.8
7.8
7.8
7.8
16
7.8
7.8
7.8
7.8
7.8
7.8
7.8
7.8
7.8
7.8
7.8
7.8
7.8
7.8
7.8
390
7.8
16
16
7.8
7.8
7.8
7.8
7.8
7.8
7.8
7.8
7.8
16
7.8
ug/kg
ug/kg
uglkg
uglkg
uglkg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugikg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
E = Qu:intitation of compound exceeded the calibration rnnge
Soils reported on a dry weight basis unless flagged with a "W"
IO(i V:1ntagc Point Driw, Cayce. South C:irolina 29033 [phone] Fax [phone]! l l \\'\\W.sht..'"::J.l)~nvironmcntal.com Page: 11 of 6 I
2
NTF-02-14
CC02001-002
Description
Lot Number
Client
OJte Received
Kubal-Furr And Associates
03/02/2001
Hun!
Surrogate Q '!/4, Recovery
I ,2-Dichlorocthane-d4 75
Tolucnc-d8 81
Bromotluorobcnzcnc 80
Footnotc(s} @ An;.ilyzcd by r-..lctrohm-Peak, Inc.
Acceptance
Linli ts
70-130
70-130
70-130
PQL = Practical quantitation limit
ND= Not ddccted at or iibovc the PQL
B =-Detected in the method blank
J = Estimated result less than the PQL
SHEALY ENVIRON~tENTALSERVICES, INC.
Run2
% Recovery
71
91
128
· Date Sampled
Matrix
Percent Solid
Acceptance
Linlits
70-I 30
70-130
70-130
03/01/2001 1030
Solid
77.1
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight basis unless fiaggcd with a "W"
106 Vantage Point Dri\C, Cayce, South Carolina 290 33 (S03) 791-9700 Fax (S03) 791-9111 \Vww.she:il)1:nvironmental.com Page: 12 of 61
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(script ion NTF-02-t4 Date Sampled 031011200 I I 030
t Number CC02001-002 Matrix Solid
Client Kubal-Furr And Associates Percent Solid 77.1 lte Recei vcd 03/021200 I
Run Analytical Method Dilution Factor Analysh Date Analyst Prep Date Prep Batch I 8270C 03103/200\ 1236 MIVK 03102/200 I 0940 2227
2 8270C 03102/200 I 1758 M\VK 03/02/200 I 0940 2227
I CAS Prep Analytical
Parameter Number Method Method Result Q PQL Units Run
Semivolatile Organic Compounds by GC/MS
Acenaphthene 83-32-9 3550B 8270C ND 420 uglkg 2
lenaphlhylene 208-96-8 3550B 8270C ND 420 ug/kg 2
thracene 120-12-7 3550B 8270C ND 420 ug/kg 2
Benzo(a )anthracene 56-55-3 3550B 8270C ND 420 uglkg 2
lnzo(a)pyrene 50-32-8 3550B 8270C ND 420 ug/kg 2
nzo(b)fluoranthene 205-99-2 3550B 8270C ND 420 uglkg 2
Benzo(g,h,i)perylene 191-24-2 3550B 8270C ND 420 ug/kg 2
lnzo(k)nuoranthene 207-08-9 3550B 8270C ND 420 uglkg 2
nzoic acid 65-85-0 3550B 8270C ND 10000 uglkg 2
Benzyl alcohol 100-51-6 3550B 8270C ND 420 uglkg 2
1 1-Biphenyl 92-52-4 3550B 8270C ND 420 uglkg
'Bromophenyl phenyl e\her 101-55-3 3550B 8270C ND 420 ug/kg 2
utyl benzyl phtha!ate 85-68-7 3550B 8270C ND 420 uglkg 2
4-Chloro-3-methy\ phenol 59-50-7 3550B 8270C ND 420 ug/kg 2
IChloroaniline 106-47-8 35508 8270C ND 420 uglkg 2
(2-Chloroethoxy)methane 111-91-1 3550B 8270C ND 420 ug/kg 2
bis(2-Chloroethyl)elher 111-44-4 3550B 8270C ND 420 uglkg 2
1(2-Chloroisopropyl)elher 108-60-1 3550B 8270C ND 420 uglkg 2
Chloronaphthalene 91-58-7 3550B 8270C ND 420 ug/kg 2
2-Chlorophenol 95-57-8 35508 8270C ND 420 uglkg 2
thlorophenyl phenyl ether 7005-72-3 3550B 8270C ND 420 uglkg 2
rysene 218-01-9 3550B 8270C ND 420 uglkg 2
Di-n-butyl phthalate 84-74-2 3550B 8270C ND 420 uglkg 2
1-n-octylphthalate 117-84-0 3550B 8270C ND 420 uglkg 2
benzo(a ,h )anthracene 53-70-3 3550B 8270C ND 420 ug/kg 2
Dibenzofuran 132-64-9 3550B 8270C ND 420 uglkg 2
12-Dichlorobenzene 95-50-1 3550B 8270C ND 420 ug/kg 2
3-Dichlorobenzene 541-73-1 3550B 8270C ND 420 ug/kg 2
1,4-Dichlorobenzene 106-46-7 35508 8270C ND 420 ug/kg 2
13'-Dichlorobenzidine 91-94-1 3550B 8270C ND 1000 uglkg 2
4-Dichlorophenol 120-83-2 3550B 8270C ND 420 uglkg 2
01ethylphthalate 84-66-2 3550B 8270C ND 420 uglkg 2
.methyl phthalate 131-11-3 3550B 8270C ND 420 uglkg 2
4-Dimethylphenol 105-67-9 3550B 8270C ND 420 ug/kg 2
4,6-Dinitro-2-methylphenol 534-52-1 3550B 8270C ND 1000 ug/kg 2
14-Dinitrophenol 51-28-5 3550B 8270C ND 1000 ug/kg 2
4-Dinitrotoluene 121-14-2 3550B 8270C ND 420 uglkg 2
2,6-0initrotoluene 606-20-2 3550B 8270C ND 420 uglkg 2
,itnote(s) @ Analyzed by il.11.'trohm-Peak, Inc.
PQL = Practical quantitation limit 8 = Detected in the method bl:uik E = Quantitation of compound exceeded the calibration range
NO-= Nut ,ktectcd o.t or above the PQL J = Estimated result less than the PQL Soils reported on a dry weight basis unless !lagged with a "W"
IE,\LY ENVIRONMENTAL SERVICES, l~C.
IO(i \';intagc Point Dri\C, Cayce, South Carolina 29033 [phone] Fax [phone] ! wv,:w.she-.il)environmentJl.com Page: 13 of 61
Description NTF-02-14
Lot Number CC02001-002
Client Kubal-Furr And Associates
Date Received
Parameter
03/02/2001
Hun
2
Analytical Method
8270C
8270C
Semivolatile Organic Compounds by GC/MS
01phenyl ether
bis(2-E thylhexyl )phthalate
Fluoranthene
Fluorene
Hexachlocobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-c,d)pyrene
lsophorone
2-Methylnaphthalene
2-Melhylphenol
3 & 4-Melhylphenol
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Naphtt1alene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Runt
Surro~atc Q '1/o Recovery
Tc1vhc11yl•d 14 92
Nitrobcnzi.::ni.::-d5 71
2-Fluoi-obiphcnyl 84
2-Fluorophcnol 68
Phenol-d5 68
2,4,6-Tribrumophcnol 71
Footnotc(s): @Analyzed by Metrohm-Pcak, Inc.
Dilution Factor
CAS
Number
101-84-8
117-81-7
206-44-0
86-73-7
116-74-1
67-68-3
77-47-4
67-72-1
193-39-5
76-59-1
91-57-6
95-48-7
106-44-5
621-64-7
66-30-6
91-20-3
86-74-4
99-09-2
100-01-6
96-95-3
66-75-5
100-02-7
67-66-5
65-01-8
106-95-2
129-00-0
120-82-1
95-95-4
86-06-2
Acceptance
Limits
30-130
30-130
30-1)0
30-1 JO
J0-130
30-130
l'QL = Practical quantitation limit 8 = Detected in the method blank
Analysis Date
0)/0)/200 I 1236
0)/02/200 t 1758
Prep Analytical
Method Method
3550B 6270C
3550B 6270C
3550B 6270C
3550B 6270C
3550B 6270C
35508 6270C
35508 6270C
3550B 6270C
3550B 6270C
35508 6270C
3550B 6270C
3550B 6270C
3550B 6270C
3550B 6270C
3550B 6270C
3550B 8270C
3550B 6270C
3550B 6270C
3550B 6270C
3550B 6270C
3550B 6270C
3550B 6270C
3550B 6270C
35508 6270C
35508 6270C
3550B 6270C
3550B 6270C
35508 8270C
35508 6270C
H.11112
'1/.1 Recovery
85
73
72
80
75
80
Date Sampled 03/01/2001 1030
tvfatrix Solid
Percent Solid 77.1
Analyst
MWK
r-.!WK
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Acceptance
Limits
)0-130
30-1 JO
JO-I JO
JO-I JO
30-IJ0
30-130
Prep Date
03/02/200 I 0940
03/02/200 I 0940
Q PQL
420
420
420
420
420
420
1000
420
420
420
420
420
650
420
420
420
420
420
420
420
420
1000
1000
420
420
420
420
420
420
Prep Hatch
2227
2227
Units
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
ug/kg
uglkg
uglkg
uglkg
ug/kg
ug/kg
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
uglkg
ug/kg
uglkg
ug/kg
ug/kg
E = Quantitation of compound exceeded the calibration range
Run
1
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
;\'!) ~ ~ot detcctcd:itor:ibovc the !'QL J = Estimated result kss than the PQL Soils reported on a dry weight basis unless fl.Jggcd with a ''W"
SflE,\LY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Driw, Cayce, South Carolina 290 33 [phone] Fax [phone] ! 11 www.she-Jl)(!nVironmental.com Page: 14 of 61
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cscription
t Number
Client
111c Received
I
l.:ameter
I GC DAI
ethylene glycol
Ethylene glycol
I
I
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I
I
I
I
I
I
I
I
I
NTF-02-14
CC02001-002
Kubal-Furr And Associates
0)/02/2001
Run Analytical Method
80158
Dilution Factor
CAS
Number
111-46-6
107-21-1
otnotc(s): @ Analyzed by Metrohm-Pi:ak, Inc.
B = lxtectt-<l in the method blank
Analysis Date
0J/02/2001 1655
Prep Analytical
Method Method
80158
80158
Date Sampled
Matrix
Percent Solid
0)/01/2001 10)0
Solid
77.1
Analyst Prep Date Prep Batch
MTR
Result Q
ND
130
PQL
65
65
Units Run
mg/kg
mg/kg
PQL = Practical quantitation limit
ND"" Not detected at or above the PQL J = Estimated result less than the PQL
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry \wight basis unless flaggi:=d with a "W"
111:t\L Y 1:~VJRO,\'.\lENTAL SERVICES, l~C.
I 0(, V.inlage Poin! DriH:. C:.iycc, South Carolina 290 33 (80 3) 791-9700 fax [phone] fl wv.w.sheal)1!nVironmental.com Page: 15 of 61
Description
Lot Number
Client
Date Received
NTF-02-14
CC02001-002
Kubal-Furr And Associates
03/02/200 I
Hun Analytical :\lethod
80158
Dilution Factor Analysis Date
0J/05/200 I 0927
Date Sampled
Matrix
Percent Solid
03/01/2001 1030
Solid
77.1
Analyst
MTR
Prep Date Prep Batch
I
I
I
Parameter
CAS
Number
Prep Analytical
Method Method Result Q PQL Units Run I
GC DAI
Methanol
Fuumotc(s) @ Analyzed by r-.lctrohm-Pc::ik, Inc.
i'QL = Practical quantitation limit
ND"" Nol dctcctcd at or .ibovc the PQL
SHEALY ENVIRONMENTAL SERVICES, INC.
67-56-1
n = D.:tectt:d in the mcthod blank
J = Estimated result less than the PQL
80158 ND 1.3 mg/kg
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry \\eight basis unless flagged with a "W"
106 Vantage Point Dri,1:, Cayce, South Carolina 29033 (S03) 791-9700 Fax [phone]! 11 www.sheal;,environmcntal.com Page: 16 of 61
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lcscriµtion
ot i'-:urnbcr
Client ttc Received
I
larameter
I Subcontracted
cehc acid
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I
I
I
I
I
t'liTF-02-14
CC02001-002
Kubal-Furr And Associates
03/02/200 I
Run Analytical Method
300.0
Dilution Factor
CAS
Number
otnote(s). @Analyzed by Metrohm-Peak, Inc.
B = Dctec1t."Cl in the method blunk
Analysis Date
OJ/031200 I 0959
Prep Analytical
Method Method
300.0
Date Sampled
Matrix
Percent Solid
03/01/2001 1030
Solid
77.1
Analyst Prep Date Prep Batch
@
Result Q PQL Units Run
700 0.39 mg/kg
!'QI."" l'rJC1ic1l qu:rntit:11ion limit
ND"' Nol detected at or above the PQL J = Estimated result less than the PQL
E = Quantitation of compound exceeded the calibration range
Soils reporicd 011 a dry \\eight basis unless flagged with a "W"
J IEALY E:\'VJRO\IMENTAL SERVICES, 1;,.:c.
I 06 Vantage Point Driw, Cayce, South G..irulin:.i 290 33 [phone] Fax [phone] www.she-al)environmcntal.com Page: 17 of 61
Description NTF-01-2 Date Sampled 03/01/2001 1100 I Lot Number CC0200I-003 Matrix Solid
Client Kubal-Furr And Associates Percent Solid 77.4
D::itc Received 03/02/2001 I
Run Analytical Method Dilution Factor Analysis Date Analyst Prep Date Prep Batch
8260B 0J/02/200 I 1541 RED I
CAS Prep Analytical
I Parameter Number Method Method Result Q PQL Units Run
Volatile Organic Compounds by GC/MS
Acetone 67-64-1 5035 82608 43 32 u9/k9 I Benzene 71-43-2 5035 82608 ND 8.0 u9/k9
Bromodichloromethane 75-27-4 5035 82608 ND 8.0 u9/k9
Bromoform 75-25-2 5035 82608 ND 8.0 u9/k9 I Bromomethane (Methyl bromide) 74-83-9 5035 82608 ND 8.0 u9/k9
2-8utanone {MEK) 78-93-3 5035 82608 ND 16 u9/k9
Carbon disulfide 75-15-0 5035 82608 ND 8.0 u9/k9 I Carbon tetrachloride 56-23-5 5035 82608 ND 8.0 u9/k9
Chlorobenzene 108-90-7 5035 82608 ND 8.0 u9/k9
Chloroethane 75-00-3 5035 82608 ND 8.0 u9/k9 I Chloroform 67-66-3 5035 82608 ND 8.0 u9/k9
Chloromethane (Methyl chloride) 74-87-3 5035 82608 ND 8.0 u9/k9
Oibromochloromethane 124-48-1 5035 82608 ND 8.0 u9/k9 I 1, 1 •Dichloroethane 75-34-3 5035 82608 ND 8.0 u9/k9
1 ,2-Dichloroethane 107-06-2 5035 82608 ND 8.0 u9/k9
1, 1-Dichloroethene 75-35-4 5035 82608 ND 8.0 u9/k9 I cis-1 ,2•0ichloroethene 156-59-2 5035 82608 ND 8.0 u9/k9
trans-1,2•Dichloroelhene 156-60-5 5035 82608 ND 8.0 u9/k9
1 ,2•Dichloropropane 78-87-5 5035 82608 ND 8.0 u9/k9 I cis-1,3-Dichloropropene 10061-01-5 5035 82608 ND 8.0 u9/kg
trans-1,3-0ichloropropene 10061-02-6 5035 82608 ND 8.0 u9/k9
1,4-0ioxane 123-91-1 5035 82608 ND 400 u9/k9 I Ethylbenzene 100-41-4 5035 82608 ND 8.0 u9/k9
2-Hexanone 591-78-6 5035 82608 ND 16 u9/k9
4 -Me th yl-2-pe n ta none 108-10-1 5035 82608 ND 16 u9/k9 I Methylene chloride 75-09-2 5035 82608 ND 8.0 u9/k9
Styrene 100-42-5 5035 82608 ND 8.0 u9/kg
1, 1,2,2-Tetrachloroethane 79-34-5 5035 82608 ND 8.0 u9/k9 I Tetrachloroethene 127-18-4 5035 82608 ND 8.0 ug/k9
Toluene 108-88-3 5035 82608 ND 8.0 ug/k9
1, 1, 1-Trichloroethane 71-55-6 5035 82608 ND 8.0 u9/k9
1, 1,2-Trichloroethane 79-00-5 5035 82608 ND 8.0 u9/k9 I Trich!oroethene 79-01-6 5035 82608 ND 8.0 u9/k9
Vinyl acetate 108-05-4 5035 82608 ND 8.0 u9/k9
Vinyl chloride 75-01-4 5035 82608 ND 16 u9/k9 I Xylenes (total) 1330-20-7 5035 82608 ND 8.0 u9/k9
I
Footnote(s): @ An::ilyzed by Mctrohm-Pcak, Inc. I !'QL = Practical quantitation limit 0 -Detected in the method blank E = Qu::intit::ition of compound exceeded the calibration r::inge
ND= Not detected .it or .ibove the f>ClL J = Estim::ited result less than the PQL Soils reported on a dry weight basis unless flagged with a "W"
SI !EALY ENVIRONi\lENTA L SERVICES, INC. I 106 Vant;ige l'nint Dri\e, Cayce, South Carolina 29033 [phone] Fax [phone] wv.w.she-Jl)environmenta!.com Page: 18 nf 61
escription
ot Number
NTF-01-2
CC02001-003
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I
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I
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I
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te Received
Kubal~Furr And Associates
03/02/200 I
Runt
Surrogate Q % Recovery
I ,2•Dichlorocthane-d4 73
To1uene-d8 81
E3romotluorobenzene 79
otnotc(s). @Analyzed by Metrohm-Peak, Inc.
Acccpluncc
Limits
70-130
70-130
70-130
PQL = Practical quant[tation limit
ND .. Nut dt:tectt:d at or above tht: PQL
B -Dctccll-d in the method blank
J = Estimated result less than the PQL
/EALY ENVIRONMENTAL SERVICES, INC.
Date Sampled
Matrix
Percent Solid
03/01/2001 1100
Solid
77.4
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry \\eight basis unless !lagged with a "W"
106 Vantage Point Dri\e, Cayce, South Carolina 29033 [phone] Fax [phone] ! I wv .. w.sheal)environmental.com Page: 19 of 61
Description NTF-01-2 Date Sampled 03/01/2001 1100 I Lot Number CC0200 I -003 Matrix Solid
Client Kubal-Furr And Associates Percent Solid 77.4
Date Received 03/02/200 I I
Run Analytical Method Dilution Factor Analysis Date Analyst Prep Date Prep Batch
8270C 03/03/200 I 1316 MWK 03/02/2001 0940 2227 I 2 8270C 03/02/2001 1834 MWK 03/02/2001 0940 2227
CAS Prep Analytical I
Parameter Number Method Method Resull Q PQL Units Run
Semivolalile Organic Compounds by GC/MS I Acenaphthene 83-32-9 3550B 8270C ND 420 ug/kg 2
Acenaphthylene 208-96-8 3550B 8270C ND 420 ug/kg 2
Anthracene 120-12-7 3550B 8270G ND 420 ug/kg 2 I Benzo(a )anthracene 56-55-3 3550B 8270G ND 420 ug/kg 2
Benzo(a)pyrene 50-32-8 3550B 8270G ND 420 ug/kg 2
Benzo(b)fluoranthene 205-99-2 3550B 8270G ND 420 ug/kg 2 I Benzo(g, h ,i)perylene 191-24-2 3550B 8270G ND 420 ug/kg 2
Benzo(k)fluoranthene 207-08-9 3550B 8270G ND 420 ug/kg 2
Benzoic acid 65-85-0 3550B 8270G ND 10000 ug/kg 2 I Benzyl alcohol 100-51-6 3550B 8270G ND 420 ug/kg 2
1.1-Biphenyl 92-52-4 3550B 8270G ND 420 ug/kg
4-Bromophenyl phenyl ether 101-55-3 3550B 8270G ND 420 ug/kg 2 I Butyl benzyl phthalate 85-68-7 3550B 8270G ND 420 ug/kg 2
4-Chtoro-3-methyl phenol 59-50-7 3550B 8270G ND 420 ug/kg 2
4-Chloroaniline 106-47-8 3550B 8270G ND 420 ug/kg 2 I bis(2-Chloroethoxy)methane 111-91-1 3550B 8270G ND 420 ug/kg 2
bis(2-Chloroethyl)ether 111-44-4 3550B 8270G ND 420 ug/kg 2
bis(2-Ch!oroisopropyl)ether 108-60-1 35508 8270G ND 420 ug/kg 2 I 2-Chloronaphthalene 91-58-7 35508 8270G ND 420 ug/kg 2
2-Chlorophenol 95-57-8 35508 8270G ND 420 ug/kg 2
4-Chlorophenyl phenyl ether 7005-72-3 3550B 8270G ND 420 ug/kg 2 I Chrysene 218-01-9 3550B 8270G ND 420 ug/kg 2
Oi-n-butyl phthalate 84-74-2 35508 8270G ND 420 ug/kg 2
Oi-n-octylph thalate 117-84-0 35508 8270G ND 420 ug/kg 2 I Dibenzo(a,h )anthracene 53-70-3 3550B 8270G ND 420 ug/kg 2
Dibenzofuran 132-64-9 35508 8270G ND 420 ug/kg 2
1,2-Dichlorobenzene 95-50-1 35508 8270G ND 420 ug/kg 2 I 1,3-Dichlorobenzene 541-73-1 35508 8270G ND 420 ug/kg 2
1,4-Dich!orobenzene 106-46-7 3550B 8270C ND 420 ug/kg 2
3 ,3' -Dichlorobenzidine 91-94-1 3550B 8270C ND 1000 ug/kg 2
2,4-Dichlorophenol 120-83-2 3550B 8270C ND 420 ug/kg 2 I Diethylphthalate 84-66-2 35508 8270G ND 420 ug/kg 2
Dimethyl phthalate 131-11-3 35508 8270G ND 420 ug/kg 2
2,4-Dimethylphenol 105-67-9 35508 8270G ND 420 ug/kg 2 I 4, 6-0initro-2-methy!pheno! 534-52-1 35508 8270G ND 1000 ug/kg 2
2,4-0initrophenol 51-28-5 35508 8270G ND 1000 ug/kg 2
2 ,4-Di nitrotoluene 121-14-2 35508 8270G ND 420 ug/kg 2 I 2, 6-Dini trotoluene 606-20-2 35508 8270C ND 420 ug/kg 2
Foot119te(s) @ Analyzed by Mctrohm-Peak, Inc. I l'QL::: Practical quamitation limit B"" Dctcctt.-d in the method blank E::: Quantitation of compound exceeded the calibration range
ND ,. Nut dctcctt:d at or above the PQL J ::: Estimated result kss than the PQL Soils reported on a dry weight basis unless nagged with a "W"
SIIEALY ENVIRONMENTAL SERVICES, INC. I IU(i Vantage Point Drive, Cnycc, South Carolina 2<J0 33 (80 3) 791-9700 Fax [phone] www.shcaljt:nvironmental.com Page: 20 of 61
NTF-01-2
CC02001-003
cscription
ot Number
lient
JtC Received
Kubal-Furr And Associates
0310212001
I
I
Parameter
Run
2
Analytical Method
8270C
8270C
Semivolatile Organic Compounds by GC/MS
Diphenyl ether
ls(2-Ethylhexyl)phthalate
luoranthene
Fluorene
lexachlorobenzene
exachlorobutadiene
Hexachlorocyclopentadiene
1•xachloroethane
deno(1,2,3-c,d)pyrene
lsophorone
IMethylnaphthalene
Methylphenol
3 & 4-Methylphenol
--Nitrosodi-n-propylamine
-Nitrosodiphenylamine
aphthalene
'Nitroaniline
Nitroaniline
Nitroani!ine
Nitrobenzene f Nitrophenol
Nitrophenol
Pentachlorophenol
lhenanthrene
henol
Pyrene
,,2,4-Trichlorobenzene
,4 ,5-T richlorophenol
2, 4, 6-Trich!orophenol
I
Runl
Surro~ate Q '1/,, Recovery
Terphcnyl-d 14 95
Nitrobenzene-d5 67
I 2-Fluorobiphenyl 80
2-F!uorophenol 68
Phcnol-d5 65
2 ,4,6-T ribromophenol 62
otnote(s). @Analyzed by Metrohm-Peak, Inc.
Dilution Factor
CAS
Number
101-84-8
117-81-7
206-44-0
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
106-44-5
621-64-7
86-30-6
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
87-86-5
85-01-8
108-95-2
129-00-0
120-82-1
95-95-4
88-06-2
Acceptance
Limits
30-130
30-130
30-JJ0
30-lJ0
30-JJ0
30-JJ0
PQL = Practical quantitation limit 8 .. Detected in the method blank
Analysh Date
031031200 I I J 16
0J/0212001 1834
Prep Analytical
Method Method
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
Run2
0/u Recovery
88
68
70
77
72
65
Date Sampled
Matrix
Percent Solid
03/01/2001 1100
Solid
Analyst
MWK
MWK
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Acceptuncc
Limits
JO-\ JO
30-IJ0
30-130
30-130
30-JJ0
JO-I JO
77.4
Prep Date
0J/02/2001 0940
0J/0212001 0940
Q PQL
420
420
420
420
420
420
1000
420
420
420
420
420
840
420
420
420
420
420
420
420
420
1000
1000
420
420
420
420
420
420
Prep Batch
2227
2227
Units
uglkg
uglkg
ug/kg
ug/kg
ug/kg
uglkg
uglkg
uglkg
uglkg
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
uglkg
ug/kg
uglkg
ug/kg
uglkg
uglkg
uglkg
uglkg
ug/kg
uglkg
uglkg
uglkg
uglkg
E = Quantitation of compound exceeded the c.ilibrn1ion range
Run
1
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
ND .. Nut detected at or above the PQL J = Estimated result less than the l'QL Soils reported on a dry weight basis unh:ss flagged with a "W"
I !EALY ENVIRONMENTAL SERVICES, INC.
l06 Vaniage Point Drive, Cayce, South Carolina 290 33 (803) 79 !•9700 Fax [phone] www.sheal)environmental.com Page: 21 of 61
Description
Lot Number
Client
Date Rccci vcd
NTF-01-2
CC02001-003
Kubal-Furr And Associates
031021200 I
Run Analytical Method
8015B
Dilution Factor Analysis Date
03/021200\ 1714
Date Sampled 0310112001 1100
Matrix Solid
Percent Solid 77.4
Analyst
MTR
Prep Date Prep Batch
I
I
I
Parameter
CAS
Number
Prep Analytical
Method Method Result Q PQL Units Run I
GC DAI
Diethylene glycol
Ethylene glycol
. Footnotc(s): @Analyzed by Mctrohm-Peak, Inc.
PQL = Practical quantitation limit
ND= Not detected at or above the PQL
SHEALY ENVIRONMENTAL SERVICES, INC.
111-46-6
107-21-1
8"" Detected in the method blank
J = Estimated result less than 1he PQL
8015B
8015B
ND
ND
64
64
mg/kg
mg/kg
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight basis unless flagged with a "W"
106 Vantage Point Dri\e, Cayce, South Carolina 29033 (80 3) 791-9700 Fax [phone] W\VW.sheal)Cnvironmental.com Page: 22 of 61
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•script ion
ot Number
tc Received
I
lrameter
I GCDAI
thanol
I
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I
I
I
I
I
I
I
I
I
i'iTF-01-2
CC0200 I -003
Kubal-Furr And Associates
03/021200 I
Run Analytical Method
80158
Dilution Factor
CAS
Number
67-56-1
otnote(s): @ Analyzed by Metrohm-Peak, Inc.
13 = [k.-tected in the method blank
Analysis Date
03/05/2001 0938
Prep Analytical
Method Method
80158
Date Sampled
Matrix
Percent Solid
03/011200 I 1100
Solid
77.4
Analyst Prep Date Prep Batch
MTR
Result Q PQL Units
ND 1.3 mg/kg
PQL = Practical quantil::i.tion limit
ND"' Not detected at or above the PC;lL J = Estimated result less than the PQL
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight b::i.sis unless flagged with a "W"
~EALY ENVIRONMENTAL $ERV ICES, INC.
106 Vantage Point Drive, Cayce, South Carolina 290 33 [phone] Fax [phone] W\.l.w.shc-.l!}environmental.com Page: 23 of 61
Run
Description
Lot Number
Client
Date Received
NTF-01-2
CC02001-003
Kubal-Furr And Associates
03/02/2001
Run Analylical Method
300.0
Dilution Factor Analysis Date
031031200 I 0959
Date Sampled
Matrix
Percent Solid
03/01/2001 1100
Solid
77.4
Analyst Prep Date Prep Batch
@
I
I
I
Parameter
CAS
Number
Prep Analytical
Method Method Result Q PQL Units Run I
Subcontracted
Acetic acid
Footnotc(s) · @ Analyzed by Metrohm-Peak, Inc.
l'QL = l'ractical qu:mtitation limit B = Detected in the method blank
ND .. Not detected at or above the PQL J = Estimated result less than the PQL
SIIEALY ENVIRONMENTAL SERVICES, INC.
300.0 ND 0.39 mg/kg
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight basis unless flagged with a "W"
!0G Vantage Point Driw, Cayce, South Carolina 290 33 [phone] Fax [phone] ! 11 www.shealJcnvironmcntal.com Page: 24 of 61
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I
cscription 1'TF-0I-IJ Date Sampled 03/01/200 I 1145
ot Number CC02001-004 Matrix Solid
Kubal-Furr And Associates Percent Solid 77.8
te Received 03/02/200 I
I Run Analytical Method Dilution Factor Analysis Date Analyst Prep Date Prep Batch
82608 03/02/200 I 1254 RED
2 82608 50 03/05/200 I I 606 RED
I CAS Prep Analytical
Parameter Number Method Method I Volatile Organic Compounds by GC/MS
Result Q PQL Units Run
Acetone 67-64-1 5035 82608 2500 1200 ug/kg 2 lnzene 71-43-2 5035 82608 ND 7.9 ug/kg
omodichloromethane 75-27-4 5035 82608 ND 7.9 ug/kg
Bromoform 75-25-2 5035 82608 ND 7.9 ug/kg
lomomethane (Methyl bromide) 74-83-9 5035 82608 ND 7.9 ug/kg
. 8ulanone (MEK) 78-93-3 5035 82608 480 16 ug/kg
Carbon disulfide 75-15-0 5035 82608 ND 7.9 ug/kg
larbon tetrachloride 56-23-5 5035 82608 ND 7.9 ug/kg
hlorobenzene 108-90-7 5035 82608 ND 7.9 ug/kg
Chloroethane 75-00-3 5035 82608 ND 7.9 ug/kg
lhloroform 67-66-3 5035 82608 ND 7.9 ug/kg
hloromethane (Methyl chloride) 74-87-3 5035 82608 ND 7.9 ug/kg
Oibromochloromethane 124-48-1 5035 82608 ND 7.9 ug/kg
'1-Dichloroethane 75-34-3 5035 82608 ND 7.9 ug/kg
2•Dichloroethane 107-06-2 5035 82608 ND 7.9 ug/kg
, 1-Dichloroethene 75-35-4 5035 82608 ND 7.9 ug/kg f -1,2-Dichloroethene 156-59-2 5035 82608 ND 7.9 ug/kg
ns•1,2•Dichloroethene 156-60-5 5035 82608 ND 7.9 ug/kg
,2-Dichloropropane 78-87-5 5035 82608 ND 7.9 ug/kg f -1,3-Dichloropropene 10061-01-5 5035 82608 ND 7.9 ug/kg
ns• 1 ,3•Dichloropropene 10061-02-6 5035 82608 ND 7.9 ug/kg
,4•Dioxane 123-91-1 5035 82608 ND 390 ug/kg
Ethylbenzene 100-41-4 5035 82608 ND 7.9 ug/kg
'Hexanone 591-78-6 5035 82608 ND 16 ug/kg
Methyl-2-pentanone 108-10-1 5035 82608 ND 16 ug/kg
Methylene chloride 75-09-2 5035 82608 ND 7.9 ug/kg
ltyrene 100-42-5 5035 82608 ND 7.9 ug/kg
, 1,2,2-Tetrachloroethane 79-34-5 5035 82608 ND 7.9 ug/kg
Tetrachloroethene 127-18-4 5035 82608 ND 7.9 ug/kg
tluene 108-88-3 5035 8260B ND 7.9 ug/kg
. 1. 1-Trich!oroethane 71-55-6 5035 82608 ND 7.9 ug/kg
1, 1,2· Trichloroethane 79-00-5 5035 82608 ND 7.9 ug/kg
lrich!oroethene 79-01-6 5035 82608 ND 7.9 ug/kg
inyl acetate 108-05-4 5035 82608 ND 7.9 ug/kg
Vinyl chloride 75-01-4 5035 82608 ND 16 ug/kg
lylenes (total) 1330-20-7 5035 82608 ND 7.9 ug/kg
otnotc(s) @ Analyzed by Metrohm-Peak, Inc.
PQl."" Practi..:ul 4uuntitation limit n -D.:tected In the method blank E = Quantit:ition of compound exceeded the c::ilibr;ition range
NI)= Not d.:to:ctcd ut ur ubuvc the PQL J = Estimated n.:sult kss than the J>QL Soils reported on a dry weight busis unless flagged with a "W"
I IEAL Y ENVIRONMENT AL SERVICES, INC.
!06 Vantage Point Drive, Cayce, South Carolina 29033 (80 3) 791•9700 Fax (803) 79 !-91 ! I www.she::il)t:nvironmental.com Page: 25 of 61
NTF-01-13
CC0200 I -004
Description
Lot Number
Client
Date Received
Kubal-Furr And Associates
03/02/2001
Runl
Surrogate Q '½, Recovery
I ,2-Dichlorocth:mc-d4 76
Tolucne-d8 80
Bromonuomb..:nzcnc 8 I
Footnotc(s) @Analyzed by Mctrohrn-Peak, Inc.
Acceptance
Limits
70-130
70-130
70-130
l'QL = Pr::ictical qu:rntitation limit
ND"" Not detected at or above the l'QL
ll -Detected in the methOO blank
J = Estimated result less than the PQL
SIIEALY ENVIRONMENTAL SERVICES, INC.
Run2
% Rcconry
80
IOI
138
Date Sampled
Matrix
Percent Solid
Acceptance
Limits
70-130
70-130
70-130
03/01/2001 I 145
Solid
77.8
E = Qu:mtitation of compound exceeded the c:ilibration range
Soils reported on a dty weight basis unless flagged with a "W"
106 Yant:ige Point Dri\c, Cayce, South C:irolina 290 33 [phone] Fa.x [phone] www.shrol)environmental.com Page: 26 of 61
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•scription NTF-01-13 Date Sampled 03/01/2001 1145
ot !\umber CC02001-004 Matrix Solid
icnt Kubal-Furr And Associates Percent Solid 77.8
tc Received 03/02/2001
I Run Analytic:il Method Dilution Factor Analysis Date Analysl Prep Date Prep Hatch
8270C 03/03/200 I 1357 MWK 03/02/200 I 0940 2227
2 8270C 03/02/200 I 1909 MWK 03/02/200 I 0940 2227
I CAS Prep Analytical
Parameter Number Method Method I Semivolatile Organic Compounds by GC/MS
Result Q PQL Units Run
Acenaphthene 83-32-9 3550B 8270C ND 420 ug/kg 2
lenaphthy!ene 208-96-8 3550B 8270C ND 420 ug/kg 2
thracene 120-12-7 3550B 8270C ND 420 ug/kg 2
Benzo(a )anthracene 56-55-3 3550B 8270C ND 420 ug/kg 2
lnzo{a)pyrene 50-32-8 3550B 8270C ND 420 ug/kg 2
nzo(b)fluoranthene 205-99-2 3550B 8270C ND 420 ug/kg 2
Benzo(g,h,i)perylene 191-24-2 3550B 8270C ND 420 ug/kg 2
lnzo(k)fluoranthene 207-08-9 3550B 8270C ND 420 ug/kg 2
nzoic acid 65-85-0 3550B 8270C ND 10000 ug/kg 2
Benzy! alcohol 100-51-6 3550B 8270C ND 420 ug/kg 2
11-Biphenyl 92-52-4 3550B 8270C ND 420 ug/kg
Bromophenyl phenyl ether 101-55-3 3550B 8270C ND 420 ug/kg 2
Butyl benzyl phthalate 85-68-7 3550B 8270C ND 420 ug/kg 2
IChloro-3-methyl phenol 59-50-7 3550B 8270C ND 420 ug/kg 2
Chloroaniline 106-47-8 3550B 8270C ND 420 ug/kg 2
bis(2-Chloroethoxy)methane 111-91-1 3550B 8270C ND 420 ug/kg 2
1(2-Chloroethyl)ether 111-44-4 3550B 8270C ND 420 ug/kg 2
(2-Chtoroisopropyl)ether 108-60-1 3550B 8270C ND 420 ug/kg 2
Chloronaphthalene 91-58-7 3550B 8270C ND 420 ug/kg 2
(hlorophenol 95-57-8 3550B 8270C ND 420 ug/kg 2
h!orophenyl phenyl ether 7005-72-3 3550B 8270C ND 420 ug/kg 2
rysene 218-01-9 35508 8270C ND 420 ug/kg 2
Di-n-butyl phthalate 84-74-2 3550B 8270C ND 420 ug/kg 2
1-n-octylphthalale 117-84-0 35508 8270C ND 420 ug/kg 2
benzo(a,h )anthracene 53-70-3 35508 8270C ND 420 ug/kg 2
Dibenzofuran 132-64-9 35508 8270C ND 420 ug/kg 2
12-Dichlorobenzene 95-50-1 35508 8270C ND 420 ug/kg 2
,3-Dichlorobenzene 541-73-1 3550B 8270C ND 420 ug/kg 2
1,4-Dichlorobenzene 106-46-7 35508 8270C ND 420 ug/kg 2
13'-Dichlorobenzidine 91-94-1 3550B 8270C ND 1000 ug/kg 2
.4-Oichlorophenot 120-83-2 3550B 8270C ND 420 ug/kg 2
Oiethylphthalate 84-66-2 3550B 8270C ND 420 ug/kg 2
lmethyl phthalate 131-11-3 3550B 8270C ND 420 ug/kg 2
-Dimethylphenol 105-67-9 3550B 8270C ND 420 ug/kg 2
4,6-Dinitro-2-methylphenol 534-52-1 3550B 8270C ND 1000 ug/kg 2
I4-Dinitrophenol 51-28-5 35508 8270C ND 1000 ug/kg 2
4-Dinitrotoluene 121-14-2 35508 8270C ND 420 ug/kg 2
2,6-Dinitrotoluene 606-20-2 3550B 8270C ND 420 ug/kg 2
otnotc(s): @Analyzed by Metrohm-Peak, Inc.
l'QL = Practic..il qu..intit..ition limit ll = DctectL-<l in the method blank E = Quantitation of compound exceeded the calibration range
NI)""' '.\:ut Jd..:~tcd at or .ibnve the PQL J == Estim:itcJ result kss th:in the PQL Soils reported on a dry weight basis unless tlaggcd with a "W"
/EALY E\VJRONMENTA L SERVICES, INC.
J O(i V..intage Point Dri\e, Cayce, South Carolina 290 33 [phone] Fax (803) 79!-9! 11 \\l\\w.shea!)t:nvironmental.com Page: 27 of 61
Description NTF-01-13 Date Sampled 03/01/200 I 1145 I Lot Number CC02001-004 Matrix Solid
Client Kubal-Furr And Associates Percent Solid 77.8
O~nc Received 03/02/2001 I
Run Analytic:il ;\fethod Dilution Factor Analysis Date Analyst Prep Dale Prep Batch
8270C 03/03/200 I 1357 MWK 03/02/200 I 0900 2227 I 2 8270C 03/02/200 I !909 MWK 03102/200 I 0900 2227
CAS Prep Analytical I
Parameter Number Method Method Result Q PQL Units Run
Semivolatile Organic Compounds by GC/MS I Diphenyl ether 101-84-8 3550B 8270C ND 420 ug/kg 1
bis(2-E thylhexyl)phthalate 117-81-7 3550B 8270C ND 420 ug/kg 2
Fluoranthene 206-44-0 3550B 8270C ND 420 ug/kg 2 I Fluorene 86-73-7 3550B 8270C ND 420 ug/kg 2
Hexachlorobenzene 118-74-1 3550B 8270C ND 420 ug/kg 2
Hexachlorobutadiene 87-68-3 3550B 8270C ND 420 ug/kg 2 I Hexachlorocyclopentadiene 77-47-4 3550B 8270C ND 1000 ug/kg 2
Hexachloroethane 67-72-1 3550B 8270C ND 420 ug/kg 2
lndeno(1,2,3-c,d)pyrene 193-39-5 3550B 8270C ND 420 ug/kg 2 I lsophorone 78-59-1 35508 8270C ND 420 ug/kg 2
2-Methylnaphthalene 91-57-6 35508 8270C ND 420 ug/kg 2
2-Methylphenol 95-48-7 35508 8270C ND 420 ug/kg 2 I 3 & 4-Methylphenol 106-44-5 35508 8270C ND 860 ug/kg 2
N-Nitrosodi-n-propy1amlne 621-64-7 35508 8270C ND 420 ug/kg 2
N-Nitrosodiphenylamine 86-30-6 35508 8270C ND 420 ug/kg 2 I Naphthalene 91-20-3 3550B 8270C ND 420 ug/kg 2
2-Nitroaniline 88-74-4 35508 8270C ND 420 ug/kg 2
3-Nitroaniline 99-09-2 3550B 8270C ND 420 ug/kg 2 I 4-Nitroaniline 100-01-6 35508 8270C ND 420 ug/kg 2
Nitrobenzene 98-95-3 3550B 8270C ND 420 ug/kg 2
2-Nitrophenol 88-75-5 35508 8270C ND 420 ug/kg 2 I 4-Nitropheno! 100-02-7 35508 8270C ND 1000 ug/kg 2
Pentachloropheno! 87-86-5 35508 8270C ND 1000 ug/kg 2
Phenanthrene 85-01-8 35508 8270C ND 420 ug/kg 2 I Phenol 108-95-2 3550B 8270C ND 420 ug/kg 2
Pyrene 129-00-0 35508 8270C ND 420 ug/kg 2
1,2,4-Trichlorobenzene 120-82-1 35508 8270C ND 420 ug/kg 2 I 2, 4, 5-T richlorophenol 95-95-4 35508 8270C ND 420 ug/kg 2
2,4,6-Trichlorophenol 88-06-2 3550B 8270C ND 420 ug/kg 2
I
llunl Acceptance Run2 Accepl:ince
Surroi.:atc Q '1/., Recovery Limits % Recovery Limits
Tcrphenyl-d 14 89 30-130 80 30-tl0 I Nitrobcnzcnc-d5 53 30-130 56 30-130
2-Fluorobipheny! 60 30-130 53 30-tl0
2-Fluorophcnol 53 30-tl0 61 30-130 I l'heno1-d5 52 30-130 58 30-130
2 .-1 ,6-Tribromophenol 61 30-130 76 30-130
Fnotnote(s) · @Analyzed by Metrohm-Peak, Inc. I PQL = Practical quantitation limit 0 = Dctcct(..'li in the method blank E = Quantitation of compound exceeded the calibration range
ND= Not dctectcd at or above the PQL J = Estimated result less than the PQL Soils reported on a dry weight basis unless flagged with a "W"
SI !EALY E\'VIRONMENTA L SERVICES, INC. I 106 Vantage Poinl Driw, Cayce, South Carolina 29033 (803) 79 l-9700 Fax [phone] ! I ,,,.v.-w.shl".1l)cnvironmental.com Page: 28 of 61
cscription
i Number
Client ltc Recci ved
I
NTF-01-13
CC02001-004
Kubal-Furr And Associates
0)/02/2001
Run Analytical Method
80158
Dilution Factor
CAS
Analysis Date
0J/02/2001 17JJ
Prep Analytical
Date Sampled
Matrix
Percent Solid
0)/01/2001 1145
Solid
77.8
Analyst Prep Date Prep Batch
MTR
lrameter Number Method Method Result Q PQL Units Run
I GC DAI
ethylene glycol
Ethylene glycol
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tnote(s) · @Analyzed by Metrohm-Pcak, Inc.
PQL = Practical quantitation limit
ND= Not detected at or above the f'C)L
EALY ENVIRO~.\.IENTA L SERVICES, INC.
111-46-6
107-21-1
13 -Detected in the method blank
J = Estimated result less than the PQL
80158 ND
80158 440
64
64
mg/kg
mg/kg
E-:: Quantitation of compound exceeded the calibration range
Soils reported on a dry weight basis unless nagged with a "W"
!06 V:intage Point Driw, Cayce, South Carolina 29033 [phone] fax [phone] www.sheal)cnvironmenta!.com Page: 29 of 61
Description
Lot Number
Client
Date Received
Parameter
GC DAI
Methanol
NTF-01-13
CC02001-004
Kubal-Furr And Associates
03/02/2001
Run Analytical Method
80150
Footnott:(s) @ Analyzed by Me1rohm-Pt:ak, Inc.
Dilution Factor
CAS
Number
67-56-1
PQL = Practical quantit:ition limit 8 = Detected in the methlxl blank
Analysis Date
0J/05/200 I 0949
Prep
Method
Analytical
Method
80158
Date Sampled
Matrix
Percent Solid
03/01/200 I 1145
Solid
77.8
Analyst
MTR
Prep Date Prep Batch
Result Q PQL Units Run
ND 1.3 mg/kg
ND=-Not detected nl or above the PQL J = Estimated result less 1han the PQL
E = Quantitation of compounJ exceeded the calibration range
Soils reported on a dry weight basis unless flagged with a "\V"
Sl IEALY ENVIRONMENTAL SERVICES, 1:--!C.
106 \':int:ige Point Driw, C:iyce, South Carolina 290 33 (SO 3) 791-9700 Fax (803) 79 !-9 ! 11 wv,w.shcal}environmcnta!.com Page: 30 of 61
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scription
t Number
tc Received
lrameter
I Subcontracted
etic acid
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I
NTF-01-13
CC02001-004
Kubal-Furr And Associates
03/02/200 I
Run Analytical Method
300.0
Dilution Factor
CAS
Number
otnote(s). @ Analyzed by Metrohm-Peak, Inc.
B = Detected in the method bl.ink
Analysis Date
031031200 I 0959
Prep Analytical
Method Method
300.0
Date Sampled
Matrix
Percent Solid
03/01/2001 I 145
Solid
77.8
Analyst Prep Date Prep Batch
@
Result Q PQL Units Run
1800 0.38 mg/kg
PQL = Practical quantitation limit
ND= Not detected at or above the PQL J = Estimated result less than the PQL
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight basis unless tlagged with a "W"
!EALY ENVIRONMENT AL SERVICES, INC.
106 Vantage Point Dri\e, Cayce, South Carolina 29033 (SO 3) 791-9700 Fax (803) 79 l-911 ! www.sh~l)environmental.com Page: 31 of 61
Description
Lot Number
Client
Date Received
NTF-03-5
CC02001-005
Kubal-Furr And Associates
03/02/2001
Run Analytical Method
82608
l 82608
Dilution Factor
50
CAS
Analysis Date
03/02/2001 IJ27
03/05/200 l 1640
Prep Analytical
Date Sampled
Matrix
Percent Solid
03/01/2001 1330
Solid
76.8
Analyst Prep Date Prep Batch
RED
RED
Parameter Number Method Method Result Q PQL Units Run
Volatile Organic Compounds by GC/MS
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane {Methyl bromide)
2-Butanone {MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
ChlorOform
Chloromethane {Methyl chloride)
Oibromochloromethane
1, 1-0ichloroethane
1,2-Dichloroethane
1, 1-0ichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-0ichloropropane
cis-1,3-Dichloropropene
trans-1 ,3-Dichloropropene
1 ,4-Dioxane
Ethylbenzene
2-Hexanone
4-Methyl-2-pentanone
Methylene chloride
Styrene
1, 1,2,2-Tetrachloroethane
. Tetrachloroethene
Toluene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
Xylenes (lolal)
Fuotnotc{s) · @ Analyzed by Mctrohm-Peak, Inc.
!'QI.= l'r:irtic:11 quantitation limit
ND= Not detecll!d at or above the PQL
Sl!Et\LY ENVIRONMENTALSERVICTS, INC.
67-64-1 5035
71-43-2 5035
75-27-4 5035
75-25-2 5035
74-83-9 5035
78-93-3 5035
75-15-0 5035
56-23-5 5035
108-90-7 5035
75-00-3 5035
67-66-3 5035
74-87-3 5035
124-48-1 5035
75-34-3 5035
107-06-2 5035
75-35-4 5035
156-59-2 5035
156-60-5 5035
78-87-5 5035
10061-01-5 5035
10061-02-6 5035
123-91-1 5035
100-41-4 5035
591-78-6 5035
108-10-1 5035
75-09-2 5035
100-42-5 5035
79-34-5 5035
127-18-4 5035
108-88-3 5035
71-55-6 5035
79-00-5 5035
79-01-6 5035
108-05-4 5035
75-01-4 5035
1330-20-7 5035
B .. DctcctL"l.i in the method blank
J = Estimated result less than the PQL
8260B 5300 1300 ugikg
8260B ND 7.6 ug/kg
8260B ND 7.6 ug/kg
8260B ND 7.6 ug/kg
82608 ND 7.6 ug/kg
82608 400 15 ug/kg
82608 ND 7.6 ug/kg
8260B ND 7.6 ug/kg
8260B ND 7.6 ug/kg
8260B ND 7.6 ug/kg
8260B ND 7.6 ug/kg
82608 ND 7.6 ug/kg
8260B ND 7.6 ug/kg
8260B ND 7.6 ug/kg
82608 ND 7.6 ug/kg
8260B ND 7.6 ug/kg
8260B ND 7.6 ug/kg
82608 ND 7.6 ug/kg
8260B ND 7.6 ug/kg
82608 ND 7.6 ug/kg
82608 ND 7.6 ug/kg
82608 ND 380 ug/kg
82608 ND 7.6 ug/kg
8260B ND 15 ug/kg
82608 ND 15 ug/kg
82608 7.8 7.6 ug/kg
8260B ND 7.6 ug/kg
82608 ND 7.6 ug/kg
8260B ND 7.6 ug/kg
82608 ND 7.6 ug/kg
8260B ND 7.6 ug/kg
8260B ND 7.6 ug/kg
8260B ND 7.6 ug/kg
82608 ND 7.6 ug/kg
82608 ND 15 ug/kg
82608 ND 7.6 ug/kg
E = Quantitation of compound exceeded the calibrntion range
Soils reported on a dry weight basis unless flagged with a "W"
10() V:.inlagc Point Dri\e, Cayce, South Carolina 29033 [phone] Fax (803).79 l :911 ! www.sheal)envimnmcntal.com Page: 32 of 61
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escription
t Number
NTF-03-5
CC02001-005
Client Kubal-Furr And Associates
03/02/2001 ttc Received
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Runt Acceptance
Surrogatr Q % Recovery Limits
I l ,2-Dich loroethane-d4 76 70-130
Toluene-d8 81 70-130
Bromofluorobenzene 80 70-130
otnotc(s): @ Analyzed by Metrohm-Peak, Inc.
PQL = Practical quantitation limit
ND= Not dl1Ccted at or above the PQL
!EALY ENVIRONMENTAL SERVICES, INC.
B .. Detected in the method blank
J = Estimated result less than the PQL
Run2
o/o Recovery
70
87
122
Date Sampled
Matrix
Percent Solid
Acceptance
Linlits
70-130
70-130
70-130
03/01/2001 1330
Solid
76.8
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight basis unless flagged with a "W"
106 Vantage Point Dri\e, Cayce. South Carolina 29033 {803) 791-9700 Fax (803) 79 !-9111 \1rww.sheal)cnvironmental.com Page: 33 of 61
Description NTF-03-5 Date Sampled 03/01/2001 1330 I Lot Number CC0200 I -005 Matrix Solid
Client Kubal-Furr And Associates Percent Solid 76.8
Date Received 03/02/2001 I
Hun Analytical Method Dilution Factor Analysis Date Analyst Prep Date Prep Batch
8270C 03/03/200 I 1437 MWK 03/02/200 I 0940 2227 I 2 8270C 03/02/200 I I 944 MWK 03/02/200 I 0940 2227
CAS Prep Analytical I Parameter Number Method Method Result Q PQL Units Run
Semivolatile Organic Compounds by GC/MS I Acenaphthene 83-32-9 35508 8270C ND 420 ug/kg 2
Acenaphthylene 208-96-8 35508 8270C ND 420 ug/kg 2
Anthracene 120-12-7 35508 8270C ND 420 ug/kg 2 I Benzo(a )anthracene 56-55-3 35508 8270C ND 420 ug/kg 2
Benzo(a)pyrene 50-32-8 35508 8270C ND 420 ug/kg 2
Benzo(b)fluoranthene 205-99-2 35508 8270C ND 420 ug/kg 2 I !
Benzo(g,h,i )perylene 191-24-2 35508 8270C ND 420 ug/kg 2
Benzo(k)fluoranthene 207-08-9 35508 8270C ND 420 ug/kg 2
Benzoic acid 65-85-0 35508 8270C ND 11000 ug/kg 2 I Benzyl alcohol 100-51-6 35508 8270C ND 420 ug/kg 2
1, 1-Biphenyl 92-52-4 35508 8270C ND 420 ug/kg
4-Bromophenyl phenyl ether 101-55-3 35508 8270C ND 420 ug/kg 2 I Butyl benzyl phthalate 85-68-7 35508 8270C ND 420 ug/kg 2
4-Chloro-3-methyl phenol 59-50-7 35508 8270C ND 420 ug/kg 2
4-Chloroaniline 106-47-8 35508 8270C ND 420 ug/kg 2 I bis(2-Chloroethoxy)methane 111-91-1 35508 8270C ND 420 ug/kg 2
bis (2-Chloroethyl )ether 111-44-4 35508 8270C ND 420 ug/kg 2
bis(2-Chloroisopropyl)ether 108-60-1 35508 8270C ND 420 ug/kg 2 I 2-Chloronaphthalene 91-58-7 35508 8270C ND 420 ug/kg 2
2-Chlorophenol 95-57-8 3550B 8270G ND 420 ug/kg 2
4-Chlorophenyl phenyl ether 7005-72-3 35508 8270C ND 420 ug/kg 2 I Chrysene 218-01-9 35508 8270G ND 420 ug/kg 2
Di-n-butyl phthalate 84-74-2 35508 8270C ND 420 ug/kg 2
Di-n-octylphthalate 117-84-0 35508 8270C ND 420 ug/kg 2 I Dibenzo(a,h)anthracene 53-70-3 35508 8270C ND 420 ug/kg 2
Dibenzofuran 132-64-9 35508 8270C ND 420 ug/kg 2
1,2-Dichlorobenzene 95-50-1 35508 8270G ND 420 ug/kg 2 I 1,3-Dichlorobenzene 541-73-1 35508 8270C ND 420 ug/kg 2
1,4-Dichlorobenzene 106-46-7 3550B 8270G ND 420 ug/kg 2
3,3'-Dichlorobenzidine 91-94-1 35508 8270C ND 1100 ug/kg 2
2,4-Dichlorophenol 120-83-2 35508 8270C ND 420 ug/kg 2 I Diethylphthalate 84-66-2 35508 8270C ND 420 ug/kg 2
Dimethyl phthalate 131-11-3 3550B 8270G ND 420 ug/kg 2
2,4-Dimethylphenol 105-67-9 35508 8270C ND 420 ug/kg 2 I 4,6-0initro-2-methylphenol 534-52-1 35508 8270C ND 1100 ug/kg 2
2,4-Dinitrophenol 51-28-5 35508 8270C ND 1100 ug/kg 2
2, 4-Dinitroto!uene 121-14-2 35508 8270C ND 420 ug/kg 2 I 2, 6-Di ni trotoluene 606-20-2 35508 8270C ND 420 ug/kg 2
Footnotc(s) @ Analyzed by i>.lc1rohm-Pcak, Inc. I !'QL = l'r~ctical quantit~tion limit B = DctectL'li in the method blank E = Quantitation of compound cxc-:cded the c~libraIion r.ingc
ND= Not detected at or above the l>()L J = Estimated result less than the PQL Soils reported on a dry weight basis unless tl:iggcd with a "W"
S\!EALY ENVIR0NMENTALSERVIO:S, INC. I I I 0() Vant:igc l'oint Driw, Cayce, South Carnlina 290 33 [phone] Fax [phone] www.she:ll;1.:nvironmrntal.com Page: 34 of 61
NTF-03-5
CC02001-005
scription
t Number
Client ltc Receivt::d
Kubal-Furr And Associates
03/02/200 I
I
I
Parameter
Run
2
Analytical Method
8270C
8270C
Semivolatile Organic Compounds by GC/MS
Dipheny! ether
1(2-Elhylhexyl)phlhalale
uoranthene
Fluorene
lxachlorobenzene
xachlorobutadIene
Hexach!orocyclopentadiene
lxachloroelhane
deno( 1.2,3-c,d)pyrene
lsophorone
IMelhylnaph\halene
Methylphenol
3 & 4-Methylphenol
INilrosodi-n-propylamine
Nitrosodiphenylamine
aphthalene
'Nilroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
INilrophenol
-Nitrophenol
Pentachlorophenol
l•nanlhrene
encl
Pyrene
,2,4-Trichlorobenzene
, 4 ,5-T rich!orophenol
2, 4 ,6-T rich!orophenol
I
Runt
Surrogate Q '1/o Recovery
Tcrphenyl-d I➔ 90
Nitrobenzene-d5 66
I 2-Fluorobiphenyl 75
2-Fluorophenol 43
Phcno1-d5 64
2,4,6-Tribromophcnol 67
otnotc(s) @Analyzed by Mdrohm-Peak, Inc.
Dilution Factor
CAS
Number
101-84-8
117-81-7
206-44-0
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
106-44-5
621-64-7
86-30-6
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
87-86-5
85-01-8
108-95-2
129-00-0
120-82-1
95-95-4
88-06-2
Acceptance
Limits
30-130
30-130
30-130
30-130
30-130
30-\J0
PQL = Practical quantitation limit 8 = Detected in the method blank
Analysis Date
03/03/2001 1437
03/02/200 I I 944
Prep Analytical
Method Method
3550B 8270C
3550B 8270C
35508 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 827DC
35508 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 827DC
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
3550B 8270C
35508 8270C
35508 8270C
H.un2
0/u Recovery
78
68
65
64
69
73
Date Sampled
ivlatrix
Percent Solid
03/01/2001 1330
Solid
Analyst
MWK
MWK
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1900
ND
ND
ND
ND
Acceptance
Lintits
JO-I JO
30-130
JO-\ 30
30-130
JO-I 30
30-130
76.8
Prep Date
03/02/2001 0940
03/02/200 I 0940
Q PQL
420
420
420
420
420
420
1100
420
420
420
420
420
860
420
420
420
420
420
420
420
420
1100
1100
420
420
420
420
420
420
Pn:p Batch
2227
2227
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
E = Quantitation of compound exceeded the calibration range
ND= Nol detected at or above the PQL J = Estimated result less than the PQL Soils reported on a dry weight basis unless nagged with a ''W"
!EALY ENVIRONMENTAL SERVICES, INC.
106 VanI:1gi: Point Dri,c, C.iycc, Sou!h Carolina 290 33 (80 3) 791-9700 fox (803) 79I-9I l l y,·wy,•,sheal)environmental.com Page: 35 of 61
Run
1
2
2
2
2
2
2
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2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
Description
Lot Number
Client
Date Received
NTF-03-5
CC02001-005
Kubal-Furr And Associates
03/02/2001
Rua Analytical Method
80158
Dilution Factor Analysis Date
0)/02/2001 1752
Date Sampled 03/01/2001 1330
Matrix Solid
Percent Solid 76.8
Analyst
MTR
Prep Date Prep Batch
I
I
I
Parameter
CAS
Number
Prep Analytical
Method Method Result Q PQL Units Run I
GC DAI
Oielhylene glycol
Ethylene glycol
Foot11ntr.:(s) @ An.ilyzcd by Mctrohm-Peak, Inc.
PQL = Practic:11 qullntit.ition limit
ND'"' Not detected lit or t1bovc the PQL
SI !EALY ENVIRON!'v1ENTAL SERVICES, INC.
111-46-6
107-21-1
D = DctcctL\.I in the method blank
J = Estimated result kss than the PQL
8015B
8015B
ND
ND
65
65
mg/kg
mg/kg
E = Quantitation of compound exceeded the c.itibration range
Soils reported on a dry weight basis unless tlaggcd with a "W"
106 V::int::igc Point Dri\1.:1 Cayce, South Carolina 29033 [phone] fax [phone] v.·ww.sheal)Cnvironmental.com P::igc: 36 of 61
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escription
ot Number
IL" Received
I
'arameter
I GCDAI
ethanol
I
I
I
I
I
I
I
I
I
I
I
I
NTF-03-5
CC02001-005
Kubal-Furr And Associates
03/02/200 I
Ru" Analytical Method
80158
Dilution Factor
CAS
Number
67-56-1
otnote(s). @Analyzed by Metrohm-Peak, Inc.
8 = D.!teckd in the method blank
Analysis Date
0J/05/2001 1000
Prep Analytical
Method Method
80158
Date Sampled
Matrix
Percent Solid
03/01/2001 1330
Solid
76.8
Analyst Prep Date Prep Batch
MTR
Result Q PQL Units
ND 1.3 mg/kg
l'QL = Practical quantitation limit
ND= Not detecled at or above the PQL J = Estimated result less than the PQL
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight basis unless nagged with a "W"
I/EALY ENVIRONME;,,,'T AL SERVICES, NC.
106 Vantage Point Drive, Cayce, South Carolina 29033 (80 3) 791-9700 Fa."< [phone] www.sheal:,environmental.com Page; 37 of 61
Run
Description
Lot Number
Client
Date Received
NTF-03-5
CC0200 I -005
Kubal-Furr And Associates
03/02/200 I
Run Analytical i\lcthod
300.0
Dilution Factor Analysi.~ Dale
0J/03/2001 0959
Date Sampled 03/01/2001 1330
Matrix Solid I
Percent Solid 76.8
I
Analyst Prep Dale Prep Balch
@ I
Parameta
CAS
Number
Prep Analytical
Method Method Result Q PQL Units Run I
Subcontracted
Acetic acid
F0ot110Le(s): @ Analyzed by Mt.!trohm-Peak, Inc.
J>QL = Practical quantitation limit
ND= N,11 d.:tc..:teJ i.lt or i.lbovc the l'()L
SIIEALY ENVIRONMENTAL SERVICES, l~C.
D = Dctect1.'(l in the method blank
J = Estimutt:tl result kss than the PQL
300.0 1900 0.39 mg/kg
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight basis unless tlaggeJ with a "W"
106 Vantage Point Dri\e, C:iyce, South C;1ro!in:i 29033 (80 3) 791-9700 Fax (803) 79 !-9 ! I! www.shcal)t:nvironmcntal.com !'age: 38 of 6!
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scription NTF-03-13 Date Sampled 03/01/2001 1405
t Number CC02001-006 Matrix Solid
Client Kubal-Furr And Associates Percent Solid 78.0 lite Recci ved 03/02/200 I
I
Run Analytical Method Dilution Factor Analysis Date Analyst Prep Date Prep Batch
82608 031021200 I 1400 RED
2 82608 50 031051200 I 1459 RED
I CAS Prep Analytical
Parameter Number Method Melhod Result Q PQL Units Run
I Volatile Organic Compounds by GC/MS
Acetone 67-64-1 5035 8260B 3600 1100 uglkg 2
lnzene 71-43-2 5035 8260B ND 7 .. 9 ug/kg
omodichloromethane 75-27-4 5035 8260B ND 7.9 ug/kg
Bromoform 75-25-2 5035 8260B ND 7.9 ug/kg
lomomethane (Methyl bromide) 74-83-9 5035 8260B ND 7.9 uglkg
Butanone (MEK) 78-93-3 5035 8260B 520 16 ug/kg
Carbon disulfide 75-15-0 5035 8260B ND 7.9 uglkg
lrbon tetrachloride 56-23-5 5035 8260B ND 7.9 ug/kg
lorobenzene 108-90-7 5035 8260B ND 7.9 ug/kg
Chloroethane 75-00-3 5035 8260B ND 7.9 uglkg
lloroform 67-66-3 5035 8260B ND 7.9 uglkg
Joromethane (Methyl chloride) 74-87-3 5035 8260B ND 7.9 ug/kg
bromochloromethane 124-48-1 5035 8260B ND 7.9 uglkg
'1-Dichloroethane 75-34-3 5035 8260B ND 7.9 uglkg
2-Dichloroethane 107-06-2 5035 8260B ND 7.9 uglkg
.1-Dichloroethene 75-35-4 5035 8260B ND 7.9 uglkg 1· 1,2-Dichloroethene 156-59-2 5035 8260B ND 7.9 uglkg
ns-1,2-Dichloroethene 156-60-5 5035 8260B ND 7.9 uglkg
,2-Dichloropropane 78-87-5 5035 8260B ND 7.9 uglkg
cis-1,3-Dichloropropene 10061-01-5 5035 8260B ND 7.9 uglkg
lns-1,3-Dichloropropene 10061-02-6 5035 8260B ND 7.9 ug/kg
.4-Dioxane 123-91-1 5035 82608 ND 400 ug/kg
Ethy!benzene 100-41-4 5035 82608 ND 7.9 uglkg
IHexanone 591-78-6 5035 8260B ND 16 uglkg
Methyl-2-pentanone 108-10-1 5035 8260B ND 16 ug/kg
Methylene chloride 75-09-2 5035 8260B 9.6 7.9 uglkg
lyrene 100-42-5 5035 8260B ND 7.9 uglkg
1,2,2-Tetrachloroethane 79-34-5 5035 82608 ND 7.9 uglkg
Tetrachloroethene 127-18-4 5035 8260B ND 7.9 uglkg
lluene 108-88-3 5035 8260B ND 7.9 uglkg
1, 1-Trichloroethane 71-55-6 5035 82608 ND 7.9 uglkg
1, 1,2-Trichloroethane 79-00-5 5035 82608 ND 7.9 uglkg
lichloroethene 79-01-6 5035 8260B ND 7.9 ug/kg
nyl acetate 108-05-4 5035 8260B ND 7.9 uglkg
Vinyl chloride 75-01-4 5035 82608 ND 16 uglkg
llenes (total) 1330-20-7 5035 8260B ND 7.9 uglkg
otnote(s) @ Analyzed by Metrohm-Peak, Inc.
PQL = Practical quantitation limit B =-Detected in the method blank E = Quantitation of compound exceeded the calibr;itlon r.mge
ND.= Not ddected at or above the PQL J = Estimated result less than the PQL Soils reported on a dry weight basis unless flagged with a "W"
!EALY ENVIRONI\IENTAL SERVICES, 17':C.
I 0(, Vant:igc Point Dri\e, C:iycc, South C:irulin:i 29033 {803) 791-9700 Fax [phone]! I I www.shca1:,i:nvironmentaLcorn Page: 39 of 61
NTF-03-13
CC02001-006
Description
Lot Number
Client
Date Recci vcd
Kubal-Furr And Associates
03/02/2001
Runl
Surro~:itl' Q '1/., Recovery
1,2-Dichloroethane-di..l 76
Tolucnc-d8 81
Bromo!luorobenzcnc 81
Fo11t11ote(s) @ Analyzed by Mctrohm-Peak, Inc.
Acceptance
Limit.~
70-130
70-130
70-130
l'QL = Practical qu:rntitation limit
ND= Not detected at or above the PQL
B = Detectt.>d in the method blank
J = Estimated result less than the PQL
SIIEAL Y ENVIRONMENTAL SERVICES, INC.
Run2
% Recovery
78
99
144
Date Sampled
Matrix
Percent Solid
Acceptance
Limits
70-130
70-130
70-130
03/01/200 I 1405
Solid
78.0
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight basis unless flagged with a "W"
I 0(, Vantage Point Driw, Cayce, South Carolina 29033 (80 3) 791-9700 Fax [phone] www.sheal)enVironmental.com Page: 40 of 61
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scription NTF-03-13 Date Sampled 0310 I 1200 I I 405
t Number CC0200 I -006 Matrix Solid
Client Kubal-Furr And Associates Percent Solid 78.0 ltc Received 03102/2001
I Run Analytical Method Dilution Factor Analysis Date Analyst Prep Date Prep Batch
8270C 031031200 I 1518 MWK 031021200 I 0940 2227
2 8270C 031021200 I 2020 MWK 031021200 I 0900 2227
I CAS Prep Analytical
Pnrnmeter Number Method Method Result Q PQL Units Run
Semivolatile Organic Compounds by GC/MS
Acenaphthene 83-32-9 3550B 8270C ND 420 ug/kg 2
lenaphthylene 208-96-8 3550B 8270C ND 420 ug/kg 2
thracene 120-12-7 35508 8270C ND 420 uglkg 2
Benzo{a )anthracene 56-55-3 35508 8270C ND 420 uglkg 2
lnzo(a)pyrene 50-32-8 35508 8270C ND 420 ug/kg 2
nzo{b)fluoranthene 205-99-2 35508 8270C ND 420 ug/kg 2
Benzo(g,h,i)perylene 191-24-2 3550B 8270C ND 420 ug/kg 2
lnzo(k)fluoranlhene 207-08-9 3550B 8270C ND 420 ug/kg 2
nzoic acid 65-85-0 35508 8270C ND 11000 ug/kg 2
Benzyl alcohol 100-51-6 3550B 8270C ND 420 ug/kg 2
-1-Biphenyl 92-52-4 3550B 8270C ND 420 ug/kg
Bromophenyl phenyl ether 101-55-3 3550B 8270C ND 420 ug/kg 2
Butyl benzyl phthalate 85-68-7 3550B 8270C ND 420 ug/kg 2
'Chloro-3'melhyl phenol 59-50-7 35508 8270C ND 420 ug/kg 2
Chloroani!ine 106-47-8 35508 8270C ND 420 uglkg 2
s(2-Chloroethoxy)methane 111-91-1 35508 8270C ND 420 ug/kg 2
1(2-Chloroelhyl)elher 111-44-4 3550B 8270C ND 420 ug/kg 2
(2-Chloroisopropyl)ether 108-60-1 3550B 8270C ND 420 ug/kg 2
Chloronaphthalene 91-58-7 3550B 8270C ND 420 ug/kg 2
2-Chlorophenol 95-57-8 3550B 8270C ND 420 ug/kg 2
lChlorophenyl phenyl elher 7005-72-3 35508 8270C ND 420 ug/kg 2
rysene 218-01-9 35508 8270C ND 420 ug/kg 2
Di-n-butyl phlhalate 84-74-2 35508 8270C ND 420 ug/kg 2
1-n-oclylphlhalate 117-84-0 35508 8270C ND 420 uglkg 2
benzo{a. h )an thracene 53-70-3 35508 8270C ND 420 ug/kg 2
Oibenzofuran 132-64-9 35508 8270C ND 420 ug/kg 2
12-Dichlorobenzene 95-50-1 3550B 8270C ND 420 ug/kg 2
3-0ich!orobenzene 541-73-1 3550B 8270C ND 420 ug/kg 2
1,4-Dich!orobenzene 106-46-7 3550B 8270C ND 420 ug/kg 2
I3'-Dichlorobenzidine 91-94-1 3550B 8270C ND 1100 ug/kg 2
4-Dichlorophenol 120-83-2 3550B 8270C ND 420 ug/kg 2
Diethylphthalate 84-66-2 35508 8270C ND 420 uglkg 2
limethyl phthalate 131-11-3 3550B 8270C ND 420 ug/kg 2
4-0imethytphenol 105-67-9 3550B 8270C ND 420 ug/kg 2
4,6-0initro-2-methylpheno! 534-52-1 3550B 8270C ND 1100 ug/kg 2
I4-Dinitrophenol 51-28-5 35508 8270C ND 1100 ug/kg 2
4-Dinitrotoluene 121-14-2 35508 8270C ND 420 ug/kg 2
2 ,6-Dinitrotoluene 606-20-2 35508 8270C ND 420 ug/kg 2
HllllOk(s) @ Analyzed by Mctrohm•Peak, tnc.
l'QL = Practic::i\ quantitation limit B = Lktectc..-d in the method blank E = Quantitation of compound exceeded the calibr::ition range
ND= Not detected at or obove the PQL J = Estimated result less than the PQL Soils reported on a dry weight basis unless flagged with a "W"
/EALY ENVJRON~IENTA L SERVICES, INC.
10() V:intagi:: Point Dri\e, Cayce, South Carolina 29033 [phone] Fax (803) 79 l-91 ! I \1;w·w.sheal)environmental.com Page: ➔I of 61
Description NTF-03-13 Date Sampled 03/01/2001 1405
Lot Number CC02001-006 Matrix Solid
Client Kubal-Furr And Associates Percent Solid 78.0
Dale Received 03/02/200 I
Run Analytical Method Dilution Factor Analysis Date Analyst Prep Date Prep Batch
8270C 03/03/2001 1518 MIVK 03/02/2001 0940 2227
2 8270C 03/02/2001 2020 MIVK 03/02/2001 0940 2227
CAS Prep Analytical
Parameter Number Method Method Result Q PQL Units Run
Semivolatile Organic Compounds by GC/MS
Oiphenyl ether 101-84-8 3550B 8270G ND 420 ug/kg
bis(2-Elhylhexyl)phthalate 117-81-7 3550B 8270G ND 420 ug/kg
Fluoranthene 206-44-0 3550B 8270G ND 420 ug/kg ·
Fluorene 86-73-7 3550B 8270G ND 420 ug/kg
Hexachlorobenzene 118-74-1 3550B 8270G ND 420 ug/kg
Hexachlorobutadiene 87-68-3 3550B 8270G ND 420 ug/kg
Hexachlorocyclopentadiene 77-47-4 3550B 8270G ND 1100 ug/kg
Hexachloroethane 67-72-1 3550B 8270C ND 420 ug/kg
lndeno(1,2,3-c,d)pyrene 193-39-5 3550B 8270G ND 420 ug/kg
lsophorone 78-59-1 3550B 8270G ND 420 ug/kg
2-Methylnaphthalene 91-57-6 3550B 8270C ND 420 ug/kg
2-Melhylphenol 95-48-7 35508 8270G ND 420 ug/kg
3 & 4-Methylphenol 106-44-5 35508 8270G ND 860 ug/kg
N-Nitrosodi-n-propylamine 621-64-7 35508 8270G ND 420 ug/kg
N-Nitrosodiphenylamine 86-30-6 35508 8270G ND 420 ug/kg
Naphthalene 91-20-3 35508 8270G ND 420 ug/kg
2-Nitroaniline 88-74-4 35508 8270G ND 420 ug/kg
3-Nitroanifine 99-09-2 3550B 8270G · ND 420 ug/kg
4-Nitroaniline 100-01-6 35508 8270G ND 420 ug/kg
Nitrobenzene 98-95-3 35508 8270G ND 420 ug/kg
2-Nitrophenol 88-75-5 3550B 8270C ND 420 ug/kg
4-Nitrophenol 100-02-7 35508 8270G ND 1100 ug/kg
Pentachlorophenol 87-86-5 35508 8270G ND 1100 ug/kg
Phenanthrene 85-01-8 35508 8270G ND 420 ug/kg
Phenol 108-95-2 35508 8270G 1500 420 ug/kg
Pyrene 129-00-0 35508 8270G ND 420 ug/kg
1,2,4-Trichlorobenzene 120-82-1 3550B 8270G ND 420 ug/kg
2,4,5-Trichlorophenol 95-95-4 3550B 8270G ND 420 ug/kg
2,4,6-Trichlorophenol 88-06-2 35508 8270G ND 420 ug/kg
Runt Acceptance Run2 Acceptance
Surrogate Q '1/., Recovery Limits 0/., Recovery Limits
Tcrphcny\-dl4 91 30-130 80 )0-130
Ni trobenzcnc-d 5 60 30-130 62 )0-130
2-Fluurobiphcnyl 69 30-130 60 J0-I30
2-Fluorophcnol 54 30-130 62 )0-130
!'hcnol-d5 58 30-130 65 30-130
2 ,4 ,6-Tribromophcnol 65 30-130 74 )0-130
Foutnotc(s): @An.:ilyzcd by Mctrohm-Pc.:ik, Inc.
B = Dctcctc<l in thc rnctho<l blank l'(.)L = Practii.:.11 quantitation lirnit
ND = Nut dctcctt:d al or a bovc the l'Q L J = Estimated n:sult less th.:in the l'QL
E = Quantitation of compound exceeded the calibration r:rngc
Soils reported on a dry weight basis unless flagged with a "W"
SI !EALY ENV!ROi-,:MENTAL SERVICES, INC.
I 0() V.1ntagc Point Dri\t:, C.:iyce, South Caiulina 290 33 (80 3) 791-9700 Fax [phone] wv.w.shcal)~nvironment.:il.com Page: 42 of 61
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
I
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11
I
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I
cscription
ot Number
1e Received
I
'arameter
I GCDAI
ethylene glycol
Ethylene glycol
I
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I
NTF-03-13
CC02001-006
Kubal-Furr And Associates
03/02/200 I
Run Analytical Method
80158
Dilution Factor
.CAS
Number
111-46-6
107-21-1
otnote(s). @ Analyzed by Metrohm-Pcak, Inc.
R = I:xteckd in the method blank
Analysis Date
0J/02/200 I 1812
Prep Analytical
Method Method
80158
80158
Date Sampled
Matrix
Percent Solid
03/0 I 1200 I 1405
Solid
78.0
Analyst Prep Date Prep Batch
MTR
Result Q
ND
ND
PQL
64
64
Units Run
mg/kg
mg/kg
PQL = Practical quantitation limit
ND= Not detected at or above the PQL J = Estimated result less than the PQL
E = Quantitation of compound exceeded the calibration range
Soi!s reported on a dry weight basis unless !lagged with a "W"
!EALY ENVIRON'.\tENTA L SERVICES, 1:-,;c.
106 \.-':1.ntagc Point Driw, Cayce, South Carolina 29033 [phone] Fax [phone] WW\\-'.she-.il}\!nvironmental.com Page: 43 of 61
Description
Lot Number
Client
Date Received
NTF-03-13
CC02001-006
Kubal-Furr And Associates
03/02/2001
R"n Analytical Method
80158
Dilution Factor Analysis Date
OJ/05/200 I IO I 2
Date Sampled
Matrix
Percent Solid
03/01/200 I 1405
Solid
78.0
Analyst
MTR
Prep Date Prep Batch
I
I
I
Parameter
CAS
Number
Prep Analytical
Method Method Result Q PQL Units Run I
GCDAI
Methanol
Fnotnote(s): @ Analyzed by Metrohm-1\:ak, Inc. ·
PQL = Pr.ictical quantitation limit
ND= Nut detected at or above the PQL
SHEALY ENVIRONMENTALSERVICTS, INC.
67-56-1
U = DctectL-<l in the method blank
J = Estimated result less than the PQL
8015B ND 1.3 mg/kg
E = Quantltation of compound exceeded the calibration range
Soils reported on a dry weight basis unkss !lagged with a "\V"
106 Vantage Point Dri\c, Cayce, South Carolina 290 33 (SO 3) 791-9700 Fax [phone] ! I www.sh1..>al)environmental.com Page: ..i.i of 61
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cscription
ot.Numbcr
tc Received
I
'arameter
l Subcontracted
etic acid
I
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I
I
I
I
I
I
I
I
NTF-03-13
CC02001-006
Kubal-Furr And Associates
03/02/200 I
Run Analytical :\-lcthod
300.0
Dilution Factor
CAS
Number
otnote(s). @Analyzed by Mctrohm-Peak, Inc.
B = Ixtected in the method blank
Analysis Date
031031200! 0959
Prep Analytical
Method Method
300.0
Date Sampled
Matrix
Percent Solid
03/0 I /200 I 1405
Solid
78.0
Analyst Prep Date Prep Batch
@
Result Q PQL Units Run
1600 0.38 mg/kg
PQL = Practical quantitation limit
ND= Not detected at or nbove the PQL J = Estimated result less than the PQL
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight basis unless tlagged with a "W"
IIEAL Y ENVIRONME,'TAL SERVICTS, INC.
I 06 Vantage Point Drive, Cayce, South Carolina 290 33 [phone] Fax [phone] y,v.w.shcal)environmental.com Page: 45 of 61
Description
Lot Number
Client
D:.itc Received
NTF-04-13
CC02001-007
Kubal-Furr And Associates
03/02/200 I
Run Analytical Method
82608
Dilution Factor Analysi.~ Date
03/02/2001 1434
Date Sampled 03/01/2001 1510
Matrix Solid
Percent Solid 75.7
Analyst
RED
Prep Date Prep Batch
I
I
I
Parameter
CAS
Number
Prep Analytical
Method Method Result Q PQL Units Run I
Volatile Organic Compounds by GC/MS
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane {Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Dibromochloromethane
1, 1-Dichloroethane
1,2-Dich!oroethane
1, 1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dich!oropropane
cis-1,3-Dichloropropene
trans-1,3-0ichloropropene
1,4-Dioxane
Ethylbenzene
2-Hexanone
4-Methyl-2-pentanone
Methylene chloride
Styrene
1, 1 ,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
. Xylenes (total)
hll1l1wti.:(s) @ Analyzed by Metrnhm-Peak, Inc.
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
123-91-1
100-41-4
591-78-6
108-10-1
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
108-05-4
75-01-4
1330-20-7
8 = O..:tcctt--d in the method bl:uik
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
5035
l'()L = /'r:ictic::d qu:rntitation limit
ND= Not detected ;.itor above the l'QL J = Estimated result less than the PQL
Sl!Er\LY ENV!RO:-.i:-.!ENTALSERVICES, 1;,.:c.
8260B ND 31 ug/kg
8260B ND 7.8 uglkg
8260B ND 7.8 ug/kg
8260B ND 7.8 ug/kg
8260B ND 7.8 uglkg
8260B ND 16 ug/kg
8260B ND 7.8 ug/kg
8260B ND 7.8 u9/kg
8260B ND 7.8 uglkg
8260B ND 7.8 uglkg
8260B ND 7.8 ug/kg
82608 ND 7.8 ug/kg
82608 ND 7.8 ugikg
82608 ND 7.8 ug/kg
82608 ND 7.8 uglkg
82608 ND 7.8 uglkg
82608 ND 7.8 uglkg
82608 ND 7.8 ug/kg
82608 ND 7.8 ug/kg
82608 ND 7.8 uglkg
82608 ND 7.8 ug/kg
82608 ND 390 ug/kg
82608 ND 7.8 ug/kg
82608 ND 16 ug/kg
82608 ND 16 uglkg
82608 12 7.8 uglkg
82608 ND 7.8 u9lk9
82608 ND 7.8 ug/kg
82608 ND 7.8 u9lk9
82608 ND 7.8 u9/kg
82608 ND 7.8 ug/kg
82608 ND 7.8 uglkg
82608 ND 7.8 ug/kg
82608 ND 7.8 uglkg
82608 ND 16 u9/k9
82608 ND 7.8 u9/k9
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight basis unless flagged with a "W"
IO(i V:.int:i.gt: Point Dri\e, Cayce, South Carolina 29033 [phone] Fa.'( (S03) 791-9111 www.shea1)envirunmental.com Page: 46 of 6!
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t Number
NTF-04-13
CC02001-007
tc Received
Kubal-Furr And Associates
03/02/200 I
H.unl
Surrogate Q %, Recovery
l ,2-Dichloroethane-d4 75
Toluene-dS 85
Bromotluorobcnzcne 81
Acceptance
Limits
70-llO
70-I JO
70-130
otnote(s): @Analyzed by Metrohm-Peak, Inc.
PQL = Practical quantitation limit
NO; Not deti:cted at or above the PQL
EALY ENVIRONMENTAL SERVICES, INC.
B = Detected in the method blank
J = Estimated result less than the PQL
Date Sampled
Matrix
Percent Solid
03/01/2001 1510
Solid
75.7
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight basis unless flagged with a "W"
106 Vantage Point Dri\e, Cayce, South Carolina 290 33 (80 3) 791-9700 Fax [phone] I 11 W\\1W.Shl·al)t:nvironmental.com Page: 47 of 61
Description NTF-04-13 Date Sampled 03/01/2001 1510 I Lot NLm1bcr CC02001-007 Matrix Solid
Client Kubal-Furr And Associates Percent 6olid 75.7
D,Hc Received 03/02/200 I I
Run Analytical Method Dilution Faclor Analysis Date Analyst Prep Date Prep Hatch
8270C 03/03/200 I 1559 MWK 03/02/2001 0900 2227 I 2 8270C 03/02/200 I 2055 ;-...1\VK 03/02/2001 0900 2227
CAS Prep Analytical I Paramder Number Method Method Result Q PQL Units Run
Somivolatile Organic Compounds by GC/MS I Acenaphthene 83-32-9 3550B 8270C ND 430 ug/kg 2
Acenaphthylene 208-96-8 3550B 8270C ND 430 ug/kg 2
Anthracene 120-12-7 3550B 8270C ND 430 ug/kg 2 I Benzo(a )anthracene 56-55-3 3550B 8270C ND 430 ug/kg 2
Benzo(a)pyrene 50-32-8 3550B 8270C ND 430 ug/kg 2
Benzo(b )fluoranthene 205-99-2 3550B 8270C ND 430 ug/kg 2 I Benzo(g ,h ,i )perylene 191-24-2 3550B 8270C ND 430 ug/kg 2
Benzo(k )fluoranthene 207-08-9 3550B 8270C ND 430 ug/kg 2
Benzoic acid 65-85-0 3550B 8270C ND 11000 ug/kg 2 I Benzyl alcohol 100-51-6 3550B 8270C ND 430 ug/kg 2
1, 1-Biphenyl 92-52-4 3550B 8270C ND 430 ug/kg
4-Bromophenyl phenyl ether 101-55-3 3550B 8270C ND 430 ug/kg 2 I Butyl benzyl phlhalate 85-68-7 3550B 8270C ND 430 ug/kg 2
4-Chloro-3-methyl phenol 59-50-7 35508 8270C ND 430 ug/kg 2
4-Chloroaniline 106-47-8 35508 8270C ND 430 ug/kg 2 I bis(2-Chloroethoxy)methane 111-91-1 3550B 8270C ND 430 ug/kg 2
bis(2-Chloroethyl )ether 111-44-4 3550B 8270C ND 430 ug/kg 2
bis(2-Chloroisopropyt )ether 108-60-1 3550B 8270C ND 430 ug/kg 2 I 2-Chloronaphthalene 91-58-7 3550B 8270C ND 430 ug/kg 2
2-Chlorophenol 95-57-8 35508 8270C ND 430 ug/kg 2
4-Chlorophenyl phenyl ether 7005-72-3 35508 8270C ND 430 ug/kg 2 I Chrysene 218-01-9 35508 8270C ND 430 ug/kg 2
Oi-n-butyl phthalate 84-74-2 3550B 8270C ND 430 ug/kg 2
Di-n-octylphthalate 117-84-0 3550B 8270C ND 430 ug/kg 2 I Dibenzo(a ,h )anthracene 53-70-3 35508 8270C ND 430 ug/kg 2
Dibenzofuran 132-64-9 3550B 8270C ND 430 ug/kg 2
1,2-Dichlorobenzene 95-50-1 35508 8270C ND 430 ug/kg 2 I 1,3-Dichlorobenzene 541-73-1 35508 8270C ND 430 ug/kg 2
1,4-Dichlorobenzene 106-46-7 35508 8270C ND 430 ug/kg 2
3,3'-Dichlorobenzidine 91-94-1 3550B 8270C ND 1100 ug/kg 2
2,4-Dichlorophenol 120-83-2 3550B 8270C ND 430 ug/kg 2 I Diethylphtha!ate 84-66-2 3550B 8270C ND 430 ug/kg 2
Dimethyl phthalate 131-11-3 3550B 8270C ND 430 ug/kg 2
2,4-Dimethylphenol 105-67-9 3550B 8270C ND 430 ug/kg 2 I 4,6-Dinitro-2-methy\phenol 534-52-1 35508 8270C ND 1100 ug/kg 2
2.4-Dinitrophenol 51-28-5 3550B 8270C ND 1100 ug/kg 2
2.4-Dinitrotoluene 121-14-2 3550B 8270C ND 430 ug/kg 2 I 2,6-Dinitrotoluene 606-20-2 3550B 8270C ND 430 ug/kg 2
Fuotnote(s). @Analyzed by l\ktrohm-Pcak, Inc. I PQL = Prac1iol quantit:ition limit B = D!tected in the method blank E = Qu:m1ita1ion of compound c.,ccedcd the c.i\ibratiun range
~[)"' ~ut dctt·ctc<l al or above !he PQL J = EstimateJ resu!l kss th:in the PQL Soils reported on a dry weight basis unless !laggi.:d wi1h a ··w"
SI ll:,\L Y E\'\'IRO:\:-.IE:-S:TA L SERVICES, I;\"(. I 106 Vant:igc Point Driw, C.1yce, South Carolina 29033 (S03) 791-9700 Fax (803) 79 l-9 l l I \\'Ww.she-.. d)environmcntal.com Page: 43 of 61
cscription
ul i\umbcr
NTF-04-13
CC020U 1-007
tc Received
Kubal-Furr And Associates
0310212001
I
I
P:J.rameter
Run
2
Analytical Method
8270C
8270C
Semivolatile Organic Compounds by GC/MS
Diphenyl ether
1(2-Elhylhexyl)phlhalale
uoranthene
Fluorene
lxachlorobenzene
xachlorobutadiene
Hexachlorocyclopentadiene
,,achloroelhane
deno(1,2,3-c,d)pyrene
tsophorone
IM_elhylnaphlhalene
Methylphenol
3 & 4-Melhylphenol
'Nilrosodi-n-propylamine
Nitrosodiphenylamine
aphthalene
'Nilroaniline
Nitroaniline
-Nitroaniline
tlrobenzene
Nitrophenol
Nitrophenol
Pentachlorophenol f enanlhrene
enol
Pyrene
,2,4-Trichlorobenzene
,4,5-Tnchlorophenol
2 ,4, 6-T richlorophenol
I
Runt
Surrogate Q 0/,, Hcco very
Terphcnyl-d\4 94
Nitrobcnzene-dS 63
I 2-Fluorobiphcnyl 77
2-Fluorophenol 65
l'hcno!-d5 60
2 ,-+,6-Tribromophcnol 60
lU[llU(c(s) @ Analyzed by l\ktrohm-Pcak, Inc.
lJilution Factor
CAS
Number
101-84-8
117-81-7
206-44-0
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
106-44-5
621-64-7
86-30-6
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
87-86-5
85-01-8
108-95-2
129-00-0
120-82-1
95-95-4
88-06-2
Acceptance
Limits
30-130
30-130
30-130
30-130
30-130
30-130
l'QL"" Practical quantitation limit l3"" Dctect<..-<l in th.: method blank
Analysis Dale
03103/200 I I 559
03102/2001 2055
Prep Analytical
Method Method
35508 8270C
35508 8270C
3550B 8270C
3550B 8270C
35508 8270C
3550B 8270C
35508 8270C
3550B 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
3550B 8270C
35508 8270C
35508 8270C
35508 8270C
35508 8270C
3550B 8270C
3550B 8270C
35508 8270C
35508 8270C
35508 8270C
3550B 8270C
35508 8270C
3550B 8270C
35508 8270C
Run1
o/., Recovery
80
65
66
73
68
63
Dote Sampled
ivlatrix
Percent Solid
03101/2001 1510
Solid
Analyst
MIVK
MWK
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Acceptance
Limits
30-130
30-130
30-130
30-130
30-130
30-1 JO
75.7
Prep Date
03102/200 I 0940
03/02/2001 0940
Q PQL
430
430
430
430
430
430
1100
430
430
430
430
430
880
430
430
430
430
430
430
430
430
1100
1100
430
430
430
430
430
430
Prep Hatch
2227
2227
Units
uglkg
ug/kg
ug/kg
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
uglkg
uglkg
ug/kg
ug/kg
uglkg
uglkg
uglkg
ug/kg
uglkg
ug/kg
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
uglkg
ug/kg
uglkg
E = Quantitation of compound cxcee_ded the calibration range
ND= Not detected al or above the PQL J"" Estimated result less than the PQL Soils reported on a dry weight basis unless flagged with a "W"
IEt\LY ENVIRONYtENTALSERVICES, INC.
I 06 Vant:ige Point Dri\e, Cayce, South Carolina 29033 [phone] Fax [phone] www.shea!)environmental.com Page: -+9 of 61
Run
1
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
Description
Lot Number
Client
Date Received
NTF-04-13
CC02001-007
Kubal-Furr And Associates
03/02/200 I
R,n Analytical Method
80158
Dilution Factor Analysis Date
03/02/200 I I 83 I
Date Sampled
Matrix
Percent Solid
03/01/2001 1510
Solid
75.7
Analyst
MTR
Prep Date Prep Batch
I
I
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Parameter
CAS
Number
Prep
Melhod
Analylical
Method Result Q PQL Units Run I
GC DAI
Oiethylene glycol
Ett1ylene glycol
Foutnotc(s) · @Analyzed by Mctrohm-Pcak, Inc.
l'QL = Practical quantitation limit
ND= N11t detected at or tibovc th't: PQL
SI !EALY ENVll{ON"~tE;-..'TA L SERVICES, 1;,.:c.
111-46-6
107-21-1
l3 -Dctectt.xl in the method blank
J = Estimnted result kss than the l'QL
80158
80158
ND
ND
66
66
mg/kg
mg/kg
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight basis unless !lagged wi1h a "W"
106 Vantage Point Dri\c, Cayce, South Carolina 29033 [phone] Fax [phone] ! I W\~W.shealJcnvironmenta!.com Page: 50 of 61
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cscription
tc Received
I
lrameter
I GC DAI
ethanol
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NTF-04-13
CC02001-007
Kubal-Furr And Associates
03/02/200 I
Run Analytical Method
8015B
Dilution Factor
CAS
Number
67-56-1
otnote(s). @Analyzed by l\.ktrohm•Peak, Inc.
B.., lxtectt:tl in the method blank
Analysis Date
0J/0512001 1023
Prep Analytical
Method Method
8015B
Date Sampled
Matrix
Percent Solid
03/01/2001 1510
Solid
75.7
Analyst Prep Date Prep Batch
MTR
Result Q PQL Units
ND 1.3 mg/kg
l'QL = Practical quanlitation limit
ND= Not detected at or above the PQL J = Estimated result kss than the PQL
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight basis unless 11aggl!d with a "W"
!EALY ENVIRO:-MENT AL SERVICES, INC.
106 Vantage Point DriH:, Cayce, South Carolina 29033 (803) 791•9700 Fax [phone] wv.w.she-.il~nvironmental.com Page: 51 of 61
Run
Description
Lot Number
Client
Date Received
NTF-04-13
CC02001-007
Kubal-Furr And Associates
03/02/200 I
Run Analytical Method
300.0
Dilution Factor Analysis Date
0310312001 0959
Date Sampled 03/01/2001 1510
Matrix Solid I
Percent Solid 75.7
I
Analyst Prep Date Prep Batch
@ I
Parameter
CAS
Number
Prep Analytical
Method Method Result Q PQL Units Run I
Subcontracted
Acetic acid
Fontnotc(s). @ Analyzed by Metrohm-Pcak, Inc.
l'QL = Practical quantita1ion limit 8"' Detected in the method blank
ND= Not detected at ur abuve the PQL J = Estimated result less than the PQL
S! IEAL Y E:\'VJRO:--:~lE;-.;TAL SERVICES, INC.
300.0 ND mg/kg
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight basis unless flagged with a "W"
\06 Vantage Point Dri\C, Cayce, South Carolin::i 290 33 [phone] Fa;,; [phone] w,.,w.sheal)environmenta!.com Page: 52 of 61
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cscription NTF-05-8 Date Sampled 0)/01/2001 1610
CC02001-008 Matrix Solid
Client Kubal-Furr And Associates Percent Solid 78.0 f tc Received 03/02/2001
I Ru" Analytical Method Dilution Factor Analysis Date Analyst Prep Date Prep Batch
82608 03/02/2001 1508 RED
larnmeter
CAS Prep Analytical
Number Method Method Result Q PQL Units Run I Volatile Organic Compounds by GC/MS
cetone 67-64-1 5035 82608 53 27 ug/kg
Benzene 71-43-2 5035 82608 ND 6.9 ug/kg
lromodichloromethane 75-27-4 5035 82608 ND 6.9 ug/kg
romoform 75-25-2 5035 82608 ND 6.9 ug/kg
Bromomethane (Methyl bromide) 74-83-9 5035 82608 ND 6.9 ug/kg
IButanone (MEK) 78-93-3 5035 82608 ND 14 ug/kg
arbon disulfide 75-15-0 5035 82608 ND 6.9 ug/kg
Carbon tetrachloride 56-23-5 5035 8260B ND 6.9 ug/kg
lhlorobenzene 108-90-7 5035 8260B ND 6.9 ug/kg
hloroethane 75-00-3 5035 8260B ND 6.9 ug/kg
Chloroform 67-66-3 5035 8260B ND 6.9 ug/kg
lhloromethane (Methyl chloride) 74-87-3 5035 8260B ND 6.9 uglkg
ibromochloromethane 124-48-1 5035 8260B ND 6.9 uglkg
1, 1-0ichloroethane 75-34-3 5035 8260B ND 6.9 uglkg
__ 2-Dichloroethane 107-06-2 5035 82608 ND 6.9 ug/kg
, 1-Dichloroethene 75-35-4 5035 8260B ND 6.9 uglkg
cis-1,2-Dich!oroethene 156-59-2 5035 8260B ND 6.9 uglkg
-ans-1,2-Dichloroethene 156-60-5 5035 8260B ND 6.9 uglkg
,2-0ichloropropane 78-87-5 5035 8260B ND 6.9 ug/kg
cis-1,3-0ichloropropene 10061-01-5 5035 8260B ND 6.9 uglkg
trans-1,3-0ichloropropene 10061-02-6 5035 8260B ND 6.9 uglkg
l-4-Dioxane 123-91-1 5035 8260B ND 340 ug/kg
thylbenzene 100-41-4 5035 8260B ND 6.9 uglkg
2-Hexanone 591-78-6 5035 8260B ND 14 ug/kg
IMelhyl-2-pentanone 108-10-1 5035 82608 ND 14 uglkg
ethylene chloride 75-09-2 . 5035 82608 8.7 6.9 uglkg
Styrene 100-42-5 5035 82608 ND 6.9 uglkg
,,1,2,2-Tetrachloroelhane 79-34-5 5035 82608 ND 6.9 uglkg
etrachloroethene 127-18-4 5035 82608 ND 6.9 uglkg
Toluene 108-88-3 5035 82608 ND 6.9 uglkg
•• 1, 1-Trichloroethane 71-55-6 5035 82608 ND 6.9 uglkg
, 1,2-Trichloroethane 79-00-5 5035 8260B ND 6.9 uglkg
Trichloroethene 79-01-6 5035 8260B ND 6.9 uglkg liny! acetate 108-05-4 5035 8260B ND 6.9 ug/kg
inyl chloride 75-01-4 5035 8260B ND 14 uglkg
Xylenes (total) 1330-20-7 5035 8260B ND 6.9 uglkg
I
OOlnOk(s) @ Analyzed by Metrohm-Peak, Inc.
PQL = Practical quantitation limit U = Dctcctt:<l in the method blank E = Quantitation of compound exceeded the calibr.ition range
ND= NQt detected ut or above the PQL J == Estimated result less than the PQL Soils reported on a diy weight basis unless nagged with a "W"
! /EALY ENVIRONMENTAL SERVICES, INC.
l 06 Vantage Point Dri\e, Cayce, South Carolina 29033 [phone] Fax [phone] wv,1w.she-al)environmental.com Page: 53 of 61
NTF-05-8
CC02001-008
Description
Lot Number
Client
Date Rccci vcd
Kubal-Furr And Associates
03/02/200 I
Runt
Su rrogatl' Q '1/u Recovery
1,2•Dichloroc1hane·d➔ 74
Tolucnc-d8 83
Bromotluorobcnzene 80
Footnotc(s) @Analyzed by Metrohm•Pcak, Inc.
Acceptance
Llnlits
70-130
70-130
70-130
PQL = Practical quantitation limit
ND= Not detected at or above the PQL
8 = Detected in the method blank
J = Estimated result less than the PQL
SIIEALY ENV!RONME;-.:TALSERVICES, L'\'C.
Date Sampled
Matrix
Percent Soild
0J/01/2001 1610
Solid
78.0
E = Quantitation of compound exceeded 1he calibration range
Soils reported on a dry weight basis unless flagged with a "\V"
lUG \'~rntagc Puint Drisc, C.1ycc, South Cam!ina 290 33 (S0J) 791•9700 fox (303) 791-91 l l www.shi:.:i.l)cnvironmen1al.com
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cscription NTF-05-8 Date Sampled 03/01/2001 1610
ot Number CC02001-008 Matrix Solid
licnt Kubal-Furr And Associates Percent Solid 78.0
ate Received 03/02/2001
I Run Analytical Method Dilution Factor Analysis Date Analyst Prep Date Prep Batch
8270C 03103/200 I 1639 MIVK 03/02/2001 0940 2227
2 8270C 0JI0J/200 I I 350 MWK 03/02/200 I 0940 2227
I CAS Prep Analytical
Paramc:"ler Number Method Method Result Q PQL Units Run I Semivolatile Organic Compounds by GC/MS
Acenaphthene 83-32-9 3550B 8270C ND 420 ug/kg 2
lcenaphthylene 208-96-8 3550B 8270C ND 420 uglkg 2
nthracene 120-12-7 3550B 8270C ND 420 ug/kg 2
Benzo(a)anthracene 56-55-3 3550B 8270C ND 420 ug/kg 2
lenzo(a)pyrene 50-32-8 3550B 8270C ND 420 ug/kg 2
·. enzo(b)fluoranthene 205-99-2 3550B 8270C ND 420 ug/kg 2
Benzo(g,h,i)perylene 191-24-2 3550B 8270C ND 420 ug/kg 2
lenzo(k)fluoranthene 207-08-9 3550B 8270C ND 420 ug/kg 2
enzoic acid 65-85-0 35508 8270C ND 10000 ug/kg 2
Benzyl alcohol 100-51-6 35508 8270C ND 420 ug/kg 2 I, 1-8iphenyl 92-52-4 35508 8270C ND 420 ug/kg 1
-..sromophenyl phenyl ether 101-55-3 35508 8270C ND 420 ug/kg 2
Butyl benzyl phthalate 85-68-7 35508 8270C ND 420 uglkg 2
,-Chloro-3-methyl phenol 59-50-7 35508 8270C ND 420 ug/kg 2
-Chloroaniline 106-47-8 35508 8270C ND 420 ug/kg 2
bis{2-Chloroethoxy)methane 111-91-1 35508 8270C ND 420 ug/kg 2
lis(2-Chloroe\hyl)elher 111-44-4 3550B 8270C ND 420 ug/kg 2
is(2-Ch!oroisopropyl}ether 108-60-1 35508 8270C ND 420 ug/kg 2
2-Chloronaphthalene 91-58-7 35508 8270C ND 420 uglkg 2
,-Chlorophenol 95-57-8 35508 8270C ND 420 uglkg 2
-Chlorophenyl phenyl ether 7005-72-3 3550B 8270C ND 420 uglkg 2
hrysene 218-01-9 35508 8270C ND 420 ug/kg 2
,i-n-bulyl phlhala\e 84-74-2 3550B 8270C ND 420 ug/kg 2
i-n-octylphthalate 117-84-0 35508 8270C ND 420 uglkg 2
ibenzo(a ,h )anthracene 53-70-3 35508 8270C ND 420 ug/kg 2
Oibenzofuran 132-64-9 35508. 8270C ND 420 ug/kg 2
, .2-Dichlorobenzene 95-50-1 3550B 8270C ND 420 ug/kg 2
,3-0ichlorobenzene 541-73-1 35508 8270C ND 420 ug/kg 2
1,4-Dichlorobenzene 106-46-7 35508 8270C ND 420 ug/kg 2
,,3'-Dichlorobenzidine 91-94-1 3550B 8270C ND 1000 ug/kg 2
,4-Dichlorophenol 120-83-2 35508 8270C ND 420 ug/kg 2
Dielhylphthalate 84-66-2 35508 8270C ND 420 ug/kg 2
limethyl phthalate 131-11-3 3550B 8270C ND 420 ug/kg 2
,4-Dimethylphenol 105-67-9 35508 8270C ND 420 ug/kg 2
4,6-Dinitro-2-methylphenol 534-52-1 35508 8270C ND 1000 ug/kg 2
•. 4-Dinitrophenol 51-28-5 35508 8270C ND 1000 ug/kg 2
,4-Dinitrotoluene 121-14-2 35508 8270C ND 420 ug/kg 2
2,6-Dinitrotoluene 606-20-2 35508 8270C ND 420 ug/kg 2
lllllll\ll\:(S) @ An:ilyzeJ by ,\lr.:truhm-Pc:ik, Inc.
PQL = Practic.il quantitation limit B =-Detectt:d in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not Jeteetcd at or above the PQL J = Estimated result less than the PQL Soils reported on a dry weight basis unless flagged with a "W"
'flE:\LY E;,,,'\'JRQ:,.;.\.tENTALSERV!CES, Ji\'C.
!06 V.intage Point Dri\.\!, Cayce, South Carolina 29033 [phone] Fax (803} 791-9111 v.,.,,..w.she-.il)Cnvironmental.com Page: 55 of 61
Description NTF-05-8 Date Sampled 03/01/2001 1610 I Lot Number CC02001-008 Matrix Solid
Client Kubal-Furr And Associates Percent Solid 78.0
Date Received 03/02/200 I I
I Run Analytical Method Dilution Factor Analysis Date Analyst Pn•p Date Prep Batch
8270C 0310312001 1639 MWK 03/02/2001 0940 2227 I I
2 8270C 031031200 I 1350 MWK 03/02/200 l 0940 2227
CAS Prep Analytical I
Parameter Number Method Method Resu!J Q PQL Units Run
Semivolatile Organic Compounds by GC/MS I Oiphenyl ether 101-84-8 35508 8270C ND 420 uglkg
bis(2-E thylhexy\ )phthalate 117-81-7 35508 8270C ND 420 uglkg 2
Fluoranthene 206-44-0 35508 8270C ND 420 ug/kg 2 I Fluorene 86-73-7 35508 8270C ND 420 uglkg 2
Hexachlorobenzene 118-74-1 35508 8270C ND 420 uglkg 2
Hexachlorobutadlene 87-68-3 35508 8270C ND 420 ug/kg 2 I Hexachlorocyclopentadiene 77-47-4 35508 8270C ND 1000 uglkg 2
Hexachloroethane 67-72-1 35508 8270G ND 420 uglkg 2
lndeno(1,2,3-c,d)pyrene 193-39-5 35508 8270G ND 420 ug/kg 2 I lsophorone 78-59-1 35508 8270G ND 420 ug/kg 2
2-Methylnaphtha!ene 91-57-6 35508 8270G ND 420 uglkg 2
2-Methylphenol 95-48-7 35508 8270G ND 420 ug/kg 2 I 3 & 4-Melhylphenol 106-44-5 35508 8270C ND 850 ug/kg 2
N-Nitrosodi-n-propylamine 621-64-7 3550B 8270G ND 420 ug/kg 2
N-Nitrosodiphenylamine 86-30-6 35508 8270G ND 420 ug/kg 2 I Naphthalene 91-20-3 35508 8270G ND 420 ug/kg 2
2-Nitroaniline 88-74-4 35508 8270G ND 420 ug/kg 2
3-Nitroaniline 99-09-2 35508 8270G ND 420 uglkg 2 I 4-Nitroaniline 100-01-6 35508 8270G ND 420 ug/kg 2
Nitrobenzene 98-95-3 35508 8270G ND 420 ug/kg 2
2-Nitrophenol 88-75-5 35508 8270C ND 420 uglkg 2 I 4-Nitrophenol 100-02-7 35508 8270C ND 1000 ug/kg 2
Pentachlorophenol 87-86-5 35508 8270G ND 1000 ug/kg 2
Phenanthrene 85-01-8 35508 8270G ND 420 ug/kg 2 I Phenol 108-95-2 35508 8270G ND 420 uglkg 2
Pyrene 129-00-0 35508 8270G ND 420 ug/kg 2
1,2,4-Trichlorobenzene 120-82-1 35508 8270C ND 420 ug/kg 2 I 2,4 ,5-Trichlorophenol 95.95.4 35508 8270G ND 420 uglkg 2
2,4,6-Trichlorophenol 88-06-2 35508 8270G ND 420 uglkg 2
I
Runt Acceptance Run2 Acceptance
Surro~atc Q '1/o Recovery Limits '1/., Recovery Limits
Tc!l)henyl-d l 4 83 30-130 80 30-130 I Nitrobcnzcnc-d5 59 30-130 69 30-130
2-Fluorobiphl.!nyl 71 30-1 JO 69 30-130
2-Fluorophcno! 60 30-1 JO 76 30-130 I Phcno1-d5 58 30-130 72 30-1 JO
2 ,4 ,6-Tribromophenol 55 30-130 74 30-130
Footnote(s): @ Analyzed by Mctrohm-Pcak, Inc. I l'QL = Practical quantitation limit B .. lktectL'll in the method blank E = Quantitation of compound exceeded the cnlibra1ion range
ND= Not detected ut or above the PQL J = Estimated result kss than the PQL Soils reported on a dry weight basis unless flagged with a "W"
SI !EALY ENVIRONMENTAL SERVICES, INC. I 106 Vantage Point Dri\e, Cayce, South Carolina 290 33 [phone] Fax [phone] ,;.·ww.sheal)~nvironmental.com Pngc: 56 of 61
l escription
ot Number
tlicnt late Received
I
larameter
I GC DAI
iethylene glycol
Ethylene glycol
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NTF-05-8
CC0200 I -008
Kulrnl-Furr And Associates
03/02/2001
Run Analytical Method
80158
Dilution Factor
CAS
Number
111-46-6
107-21-1
ootnote(s) @Analyzed by Mctrohm-Peak, Inc.
8 = I:ktccted in the method blank
Analysis Date
03/02/200 I I 850
Prep Analytical
Method Method
8015B
8015B
Date Sampled
Matrix
Percent Solid
03/01/2001 1610
Solid
78.0
Analyst Prcr Date Prep Batch
MTR
Result Q
ND
ND
PQL
64
64
Units Run
mg/kg
mg/kg
l'QL = Practical qu.intiiation limit
ND = Not detected .i l or a bovc the PQ L J = Estimated result less than the PQL
E = Quantitation of compound exceeded the calibrntion range
Soils reported on a dry weight basis unless flagged with a "W"
Jll:r\LY ENY!RONMENTAL SERVICES, INC.
106 Vantage Point Driw, Cayce, South Carolina 290 33 [phone] Fa.\ [phone] v.wv.r.shea!)t:nvironmental.com Page: 57 of 61
)cscription
~ot Number
=:licnt
)ate Received
)arameter
GCDAI
·:!ethanol
i'>TF-05-8
CC0200 I -008
Kubal-Furr And Associates
03/02/2001
Run Analyticnl Method
80158
Fu1Jt11ot..:(s) @ Analyzed by Mctrohm-Pe::ik, Inc.
Dilution Factor
CAS
Number
67-56-1
PQL = Practical quantitation limit B • Dc1ect1-"<l In the method blank
Analysis Date
03/05/2001 1034
Prep Analytical
Method Method
8015B
Date Sampled
Matrix
Percent Solid
03/01/2001 1610
Solid
78.0
Analyst Prep Date Prep Batch
MTR
Result Q PQL Units Run
ND 1.3 mg/kg
ND= Not d<.:t<.:r.:t<.:d .it or a bun: th.:: I'() L J = Estimated result kss than th.: PQL
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight basis unlt:ss flagged with a "W"
.) I !EALY ENVIRO;--!MENTA L SER\' ICES, INC.
I 06 Vantage Point Driw, C::iycc, South Carolina 290 33 (80 3) 791-9700 Fax (803) 79 !-9 l I I v.ww.sheal)t:nvironmcnt.il.com Page: 58 of 61
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tcscriµtion Trip Blank Date Sampled 03/0 I /200 I 0000
or Number CC02001-009 Matrix Aqueous
Client Kubal-Furr And Associates I ate Received 03/02/2001
Run Analytical Method Dilution Factor Analysis Date Analyst Prep Date Prep Batch
I 82608 0J/051200I 124➔ RED
l)armm:ter
CAS Prep Analytical
Number Method Method Result Q PQL Units Run I Volatile Organic Compounds by GC/MS
cetone 67-64-1 50308 82608 ND 20 ug/L
Benzene 71-43-2 50308 82608 ND 5.0 ug/L
,,omodichloromethane 75-27-4 50308 8260B ND 5.0 ug/L
romoform 75-25-2 5030B 8260B ND 5.0 ug/L
Bromomethane (Methyl bromide) 74-83-9 5030B 8260B ND 5.0 ug/L
·1-Butanone (MEK) 78-93-3 5030B 8260B ND 10 ug/L
arbon disulfide 75-15-0 5030B 8260B ND 5.0 ug/L
Carbon tetrachloride 56-23-5 5030B 8260B ND 5.0 ug/L
'hlorobenzene 108-90-7 5030B 8260B ND 5.0 ug/L
hloroethane 75-00-3 5030B 8260B ND 5.0 ug/L
hloroform 67-66-3 5030B 8260B ND 5.0 ug/L
-htoromethane (Methyl chloride) 74-87-3 5030B 8260B ND 5.0 ug/L
ibromochloromethane 124-48-1 5030B 8260B ND 5.0 ug/L
, 1-Dichloroethane 75-34-3 5030B 8260B ND 5.0 ug/L
1,2-Dichloroethane 107-06-2 5030B 8260B ND 5.0 ug/L I· 1-Dichloroethene 75-35-4 5030B 8260B ND 5.0 ug/L
is-1,2-Dichtoroethene 156-59-2 5030B 8260B ND 5.0 ug/L
trans-1,2-Oichloroethene 156-60-5 5030B 8260B ND 5.0 ug/L
,.2-Dichloropropane 78-87-5 5030B 8260B ND 5.0 ug/L
is-1 ,3-Dichloropropene 10061-01-5 5030B 8260B ND 5.0 ug/L
trans-1,3-Dichloropropene 10061-02-6 5030B 8260B ND 5.0 ug/L
,,4-Dioxane 123-91-1 50308 8260B ND 250 uglL
thylbenzene 100-41-4 5030B 8260B ND 5.0 ug/L
2-Hexanone 591-78-6 5030B 8260B ND 10 ug/L
IMethyl-2-pentanone 108-10-1 5030B 8260B ND 10 ug/L
ethylene chloride 75-09-2 5030B 8260B ND 5.0 ug/L
Styrene 100-42-5 5030B 8260B ND 5.0 ug/L
•. 1,2,2-Tetrachloroethane 79-34-5 5030B 8260B ND 5.0 ug/L
etrachloroethene 127-18-4 5030B 8260B ND 5.0 uglL
Toluene 108-88-3 5030B 8260B ND 5.0 ug/L
•• 1, 1-Trichloroethane 71-55-6 50308 8260B ND 5.0 ug/L
,1,2-Trichloroethane 79-00-5 5030B 8260B ND 5.0 ug/L
Trichloroethene 79-01-6 5030B 8260B ND 5.0 ug/L linyl acetate 108-05-4 5030B 8260B ND 5.0 ug/L
inyt chloride 75-01-4 5030B 8260B ND 2.0 ug/L
Xylenes (total) 1330-20-7 5030B 8260B ND 5.0 ug/L
I
!'QL = l'ractical quantitation lirnit B"" Dctect~'O in the mcthod blank E = Quantitation of compound e.xcceded the ca!ibr.ition range
ND = Not detected at or above the PQL J = Estimated result less than !he PQL Soils reported on a dry weight basis unless flagged with a "W"
Iii \EALY ENVIRONMENTAL SERVICES, INC. l)(J \';.111tag..: l'uint Driw, Cayce, South Carolin;:i 29033 {803) 791-9700 Fa:-.. (803) 791-91 l I www.sht.".ll)1.'nvironmcnta!.com Page: 60 of 61
Trip Blank
CC02001-009
Description
Lot Number
Client
D:.i.tc Received
Kubal-Furr And Associates
03/02/200 I
Surro~:ite
! ,2-Dichloroethane-d4
Toluene-dB
Bromonuorobcnzene
PQL = Practical quantitation limit
ND= Not detected at or t1bovc the PQL
Q
SIIEALY ENVIRONMENTAL SERVICES, INC.
Hun! Acceptance
'1/,, Recovery Limits
76 70-1 J0
87 70-1]0
8] 70-1]0
B = Dcteck<l in the method bhmk
J = Estimated result kss than the PQL
Dote Somplcd
Matrix
03/01/200 I 0000
Aqueous
E = Quantitation of compound exceeded the calibration range
Soils reported on a dry weight basis unless flagged with a "W"
106 Vantage Point Dri\c, Cayce, South Carolina 290 33 [phone] Fax (803) 79 l-9 ! 11 www.sheal)\:nvironmental.com Page: 61 of 61
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Quality Control Summary
Volatiles
Method 8260B
Analysis Date: 03/02/01
Analytical Batch ID: 3MAR0201
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FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
BLK030201
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.: SAS No.: SDG No.: 3MAR0201
Matrix: (soil/water) SOIL Lab Sample ID: BLK030201
Sample wt/vol:
Level: (low/med)
5.0 (g/mL) G
LOW
Lab File ID: BLK-1
Date Received:
% Moisture: not dee.
GC Column: RTX-502.2 ID: 0.53 (mm)
Date Analyzed: 03/02/01
Dilution Factor: 1.0
Soil Extract Volume: (mL) ----.Soil Aliquot Volume: ____ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
75-71-8---------Dichlorodifluoromethane 5.0000 u
74-87-3---------Chloromethane 5.0000 u
75-01-4---------Vinyl chloride 2.0000 u
74-83-9---------Bromomethane 5.0000 u
75-00-3---------Chloroethane 5.000.0 u
75-69-4---------Trichlorofluoromethane 5.0000 u
107-02-8--------Acrolein 50.0000 u
75-35-4---------1,1-Dichloroethene 5.0000 u
75-09-2---------Methylene chloride 5.0000 u
107-13-1--------Acrylonitrile 50.0000 u
1634-04-4-------tert-Butyl methyl ether(MTBE 5.0000 u
156-60-5--------trans-l,2-Dichloroethene 5.0000 u --75-34-3---------1,1-Dichloroethane 5.0000 u
78-93-3---------2-Butanone (MEK) 10.0000 u
67-66-3---------Chloroform 5.0000 u
74-97-5---------Bromochloromethane 5.0000 u
71-55-6---------1,1,1-Trichloroethane 5.0000 u
56-23-5---------Carbon tetrachloride 5.0000 u
107-06-2--------1,2-Dichloroethane 5.0000 u
71-43-2---------Benzene 5.0000 u
79-01-6---------Trichloroethene 5.0000 u
78-87-5---------1,2-Dichloropropane 5.0000 u
75-27-4---------Bromodichloromethane 5.0000 u
110-75-8--------2-Chloroethylvinyl ether 10.0000 u
10061-01-5------cis-l,3-Dichloropropene --5.0000 u
108-88-3--------Toluene 5.0000 u
10061-02-6------trans-l,3-Dichloropropene 5.0000 u
79-00-5---------1,1,2-Trichloroethane --5.0000 u
127-18-4--------Tetrachloroethene 5.0000 u
124-48-1--------Dibromochloromethane 5.0000 u
106-93-4--------1,2-Dibromoethane (EDB) 5.0000 u
108-90-7--------Chlorobenzene 5.0000 u
100-41-4--------Ethylbenzene 5.0000 u
FORM I VOA
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
BLK030201
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.:
Matrix: (soil/water) SOIL
SAS No.: SDG No.: 3MAR0201
Lab Sample ID: BLK030201
Sample wt/vol:
Level: (low/med)
5.0 (g/mL) G
LOW
Lab File ID:
Date Received:
BLK-1
% Moisture: not dee.
GC Column: RTX-502.2 ID: 0.53 (mm)
Date Analyzed: 03/02/01
Dilution Factor: 1.0
Soil Extract Volume: (mL) ----Soil Aliquot Volume: ____ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-38-3--------m+p-Xylenes 5.0000 u
95-47-6---------o-Xylene 5.0000 u
75-25-2---------Bromoform 5.0000 u
79-34-5---------1,1,2,2-Tetrachloroethane 5.0000 u --541-73-1--------1,3-Dichlorobenzene 5.0000 u
106-46-7--------1,4-Dichlorobenzene 5.0000 u
95-50-1---------1,2-Dichlorobenzene 5.0000 u
91-20-3---------Naphthalene 5.0000 u
67-64-1---------Acetone 20.0000 u
75-05-8---------Acetonitrile 50.0000 u
74-88-4.---------Methyl iodide 5.0000 u
107-05-1--------Allyl chloride 5.0000 u
75-15-0---------Carbon disulfide 5.0000 u
108-05-4--------Vinyl acetate 5.0000 u
107-12-0--------Propionitrile 50.0000 u
156-59-2--------cis-l,2-Dichloroethene 5.0000 u
126-98-7--------Methacrylonitrile 5.0000 u
80-62-6---------Methyl methacrylate 5.0000 u
74-95-3---------Dibromomethane 5.0000 u
108-10-1--------4-Methyl-2-pentanone 5.0000 u
97-63-2---------Ethyl methacrylate 5.0000 u
591-78-6--------2-Hexanone 10.0000 u
630-20-6--------1,l,l,2-Tetrachloroethane __ 5.0000 u
100-42-5--------Styrene 5.0000 u
96-18-4---------1,2,3-Trichloropropane 5.0000 u
110-57-6--------trans-l,4-Dichloro-2-butene_ 5.0000 u
100-44-7--------Benzyl chloride 5.0000 u
96-12-8---------1,2-Dibromo-3-chloropropane 5.0000 u
108-20-3--------Diisopropyl ether -5.0000 u
78-83-1---------Isobutyl alcohol 50.0000 u
123-91-1--------1,4-Dioxane 250.0000 u
95-63-6---------1,2,4-Trimethylbenzene 5.0000 u
108-67-8--------1,3,5-Trimethylbenzene 5.0000 u
FORM I VOA
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FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
BLK030201
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.: SAS No.: SDG No.: 3MAR0201
Matrix: (soil/water) SOIL
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) G
LOW
GC Column: RTX-502.2 ID: 0.53 (mm)
Soil Extract Volume: (mL) ----
Lab Sample ID: BLK030201
Lab File ID: BLK-1
Date Received:
Date Analyzed: 03/02/01
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
1330-20-7-------Xylene (total) 5.0000 u
76-13-1---------Freon 113 5.0000 u
60-29-7---------Ether 5.0000 u
142-28-9--------1,3-Dichloropropane 5.0000 u
594-20-7--------2,2-Dichloropropane 5.0000 u
563-58-6--------1,l-Dichloropropene 5.0000 u
108-94-1--------Cyclohexanone 50.0000 u
78-00-2---------Tetraethyllead 5.0000 u
141-78-6--------Ethyl acetate 5.0000 u
126.-99-8-- - - - - --Chloroprene 5.0000 u
FORM I VOA
FORM 2
SOIL VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.: SAS No.: SDG No.: 3MAR0201
Level: (low/med) LOW
page 1 of 1
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CLIENT
SAMPLE NO.
============ BLK030201
BLK030201LCS
BLK030201LCS
SMCl SMC2
(DCE) # (TOL)#
=:;:==== ======
74 82
71 82
74 82
SMC3 OTHER TOT
(BFB) # OUT
====== ====== ---
81 0
80 0
82 0
-
-
-
--
--
-
-
-
-
--
---
-
-
-
-
-
-
--
-
-
-
-
-
-
-
SMCl
SMC2
SMC3
(DCE)
(TOL)
(BFB)
QC
= 1,2-Dichloroethane-d4
LIMITS
(70-130)
(70-130)
(70-130)
= Toluene-dB
= Bromofluorobenzene
# Column to be used to flag recovery values
* Values outside of contract required QC limits
D System Monitoring Compound diluted out
FORM II VOA
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FORM 3
SOIL VOLATILE LAB CONTROL SAMPLE
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.: SAS No.: SDG No.: 3MAR0201
Matrix Spike -Sample No.: blk030201 Level: (low/med) LOW
SPIKE SAMPLE LCS LCS
ADDED CONCENTRATION CONCENTRATION %
COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC #
---------------------------------:;;:============ -------------===::===
1,1-Dichloroethene 50.0000 0.0000 44.3714 89
Methylene chloride 50.0000 0.0000 44.5967 89
trans-1,2-Dichloroethen 50.0000 0.0000 45.5965 91
1, 1-Dichloroethane ' 50.0000 0.0000 44.5962 89
Chloroform 50.0000 0.0000 44.3715 89
1,1,1-Trichloroethane 50.0000 0.0000 45.5071 91
Carbon tetrachloride 50.0000 0.0000 45.9959 92
1,2-Dichloroethane 50.0000 0.0000 45.0867 90
Benzene 50.0000 0.0000 44.7573 90
Trichloroethene 50.0000 0.0000 46.5236 93
1,2-Dichloropropane 50.0000 0.0000 44.2441 88
Bromodichloromethane 50.0000 0.0000 44.4730 89
cis-1,3-Dichloropropene 50.0000 0.0000 45.3502 91
Toluene 50.0000 0.0000 46.7876 94
trans-1,3-Dichloroprope 50.0000 0.0000 46.4515 93
1,1,2-Trichloroethane 50.0000 0.0000 46.0734 92
Tetrachloroethene 50.0000 0.0000 48.8154 98
Dibromochloromethane 50.0000 0.0000 46.5570 93
Chlorobenzene 50.0000 0.0000 47.6033 95
Ethylbenzene 50.0000 0.0000 50.2310 100
Bromoform 50.0000 0.0000 44.7430 89
1,1,2,2-Tetrachloroetha 50.0000 0.0000 40.6667 81
1,3-Dichlorobenzene 50.0000 0.0000 46.2227 92
1,4-Dichlorobenzene 50.0000 .0. 0000 46.0896 92
1,2-Dichlorobenzene 50.0000 0.0000 46.3360 93
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
COMMENTS:
page 1 of 2 FORM III VOA
QC.
LIMITS
REC.
======
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
FORM 3
SOIL VOLATILE LAB CONTROL SAMPLE
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code : Case No. : SAS No.: SDG No.: 3MAR0201
Matrix Spike -Sample No.: blk030201 Level: (low/med) LOW
SPIKE LCSD LCSD
ADDED CONCENTRATION % % QC LIMITS
COMPOUND (ug/Kg) (ug/Kg) REC# RPD # RPD
---------------------------------============= =====:;;: ====== ======
1,1-Dichloroethene 50.0000 43.3491 87 2 20
Methylene chloride 50.0000 44.5137 89 0 20
trans-1,2-Dichloroethen 50.0000 44.9059 90 1 20
1,1-Dichloroethane 50.0000 44 .1383 88 1 20
Chloroform 50.0000 43.9565 88 1 20
1,1,1-Trichloroethane 50.0000 44.7601 90 1 20
Carbon tetrachloride 50.0000 46.0405 92 0 20
1,2-Dichloroethane 50.0000 46.1196 92 2 20
Benzene 50.0000 45.0258 90 0 20
Trichloroethene 50.0000 46.4525 93 0 20
1,2-Dichloropropane 50.0000 44.8111 90 2 20
Bromodichloromethane 50.0000 44.8637 90 1 20
cis-1,3-Dichloropropene 50.0000 45.7846 92 1 20
Toluene 50.0000 46.8324 94 0 20
trans-1,3-Dichloroprope 50.0000 47.5372 95 2 20
1,1,2-Trichloroethane 50.0000 47.4305 95 3 20
Tetrachloroethene 50.0000 47.3205 95 3 20
Dibromochloromethane 50.0000 47.7735 96 3 20
Chlorobenzene 50.0000 47.3908 95 0 20
Ethylbenzene 50.0000 49.9583 100 0 20
Bromoform 50.0000 47.2515 94 5 20
1,1,2,2-Tetrachloroetha 50.0000 42.6409 85 5 20
1,3-Dichlorobenzene 50.0000 45.3430 91 1 20
1,4-Dichlorobenzene 50.0000 45.5392 91 1 20
1,2-Dichlorobenzene 50.0000 46.6551 93 0 20
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: 0 out of 25 outside limits
Spike Recovery: 0 out of 50 outside limits
COMMENTS:
page 2 of 2 FORM III VOA
REC.
======
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
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Quality Control Summary
Volatiles
Method 8260B
Dilutions
Analysis Date: 03/05/01
Analytical Batch ID: 3MAR0501
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FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MB030501
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.: SAS No.: SDG No.: 3MAR0501
Matrix: (soil/water) SOIL Lab Sample ID: MB030501
Sample wt/vol: 5.0 (g/mL) G
HIGH
Lab File ID: METHBLKX
Level: (low/med) Date Received:
% Moisture: not dee. Date Analyzed: 03/05/01
Dilution Factor: 50.0 GC Column: RTX-502.2 ID: 0.53 (mm)
Soil Extract Volume: (mL) ----Soil Aliquot Volume: ____ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
75-71-8---------Dichlorodifluoromethane 250.0000 u
74-87-3---------Chloromethane 250.0000 u
75-01-4---------Vinyl chloride 250.0000 u
74-83-9---------Bromomethane 250.0000 u
75-00-3---------Chloroethane 250.0000 u
75-69-4---------Trichlorofluoromethane 250.0000 u
107-02-8--------Acrolein 2500.0000 u
75-35-4---------1,1-Dichloroethene 250.0000 u
75-09-2---------Methylene chloride 250.0000 u
107-13-1--------Acrylonitrile 2500.0000 u
1634-04-4-------tert-Butyl methyl ether(MTBE 250.0000 u
156-60-5--------trans-l,2-Dichloroethene 250.0000 u ~-75-34-3---------1,1-Dichloroethane 250.0000 u
78-93-3---------2-Butanone (MEK) 500.0000 u
.67-66-3---------Chloroform 250.0000 u
74-97-5---------Bromochloromethane 250.0000 u
71-55-6---------1,1,1-Trichloroethane 250.0000 u
56-23-5---------Carbon tetrachloride 250.0000 u
107-06-2--------1,2-Dichloroethane 250.0000 u
71-43-2---------Benzene 250.0000 u
79-01-6---------Trichloroethene 250.0000 u
78-87-5---------1,2-Dichloropropane 250.0000 u
75-27-4---------Bromodichloromethane 250.0000 u
110-75-8--------2-Chloroethylvinyl ether 500.0000 u
10061-01-5------cis-l,3-Dichloropropene 250.0000 u
108-88-3--------Toluene 250.0000 u
10061-02-6------trans-l,3-Dichloropropene 250.0000 u
79-00-5---------1,1,2-Trichloroethane -250.0000 u
127-18-4--------Tetrachloroethene 250.0000 u
124-48-1--------Dibromochloromethane 250.0000 u
106-93-4--------1,2-Dibromoethane (EDB) 250.0000 u
108-90-7--------Chlorobenzene 250.0000 u
100-41-4--------Ethylbenzene 250.0000 u
FORM I VOA
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MB030501
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.:
Matrix: (soil/water) SOIL
SAS No.: SDG No.: 3MAR0501
Lab Sample ID: MB030501
Sample wt/vol: 5.0 (g/mL) G
HIGH
Lab File ID: METHBLKX
Level: (low/med) Date Received:
% Moisture: not dee.
GC Column: RTX-502.2 ID: 0.53 (mm)
Date Analyzed: 03/05/01
Dilution Factor: 50.0
Soil Extract Volume: (mL) ---Soil Aliquot Volume: ____ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-38-3--------rn+p-Xylenes 250.0000 u
95-47-6---------o-Xylene 250.0000 u
75-25-2---------Bromoforrn 250.0000 u
79-34-5---------1,1,2,2-Tetrachloroethane --250.0000 u
541-73-1--------1,3-Dichlorobenzene 250.0000 u
106-46-7--------1,4-Dichlorobenzene 250.0000 u
95-50-1---------1,2-Dichlorobenzene 250.0000 u
91-20-3---------Naphthalene 250.0000 u
67-64-1---------Acetone 1000.0000 u
75-05-8---------Acetonitrile 2500.0000 u
74-88-4---------Methyl iodide 250.0000 u
107-05-1--------Allyl chloride 250.0000 u
75-15-0---------Carbon disulfide 250.0000 u
108-05-4--------Vinyl acetate 250.0000 u
107-12-0--------Propionitrile 2500.0000 u
156-59-2--------cis-l,2-Dichloroethene 250.0000 u
126-98-7--------Methacrylonitrile 250.0000 u
80-62-6---------Methyl rnethacrylate 250.0000 u
74-95-3---------Dibromornethane 250.0000 u
108-10-1--------4-Methyl-2-pentanone 500.0000 u
97-63-2---------Ethyl rnethacrylate 250.0000 u
591-78-6--------2-Hexanone 500.0000 u
630-20-6--------1,l,l,2-Tetrachloroethane 250.0000 u --100-42-5--------Styrene 250.0000 u
96-18-4---------1,2,3-Trichloropropane 250.0000 u
110-57-6--------trans-l,4-Dichloro-2-butene 250.0000 u -100-44-7--------Benzyl chloride 250.0000 u
96-12-8---------1,2-Dibrorno-3-chloropropane 250.0000 u
108-20-3--------Diisopropyl ether -250.0000 u
78-83-1---------Isobutyl alcohol 2500.0000 u
123-91-1--------1 4-Dioxane 12500.0000 u
95-63-6---------1'2 4-Trimethylbenzene 250.0000 u ' ' 108-67-8--------1,3,5-Trimethylbenzene 250.0000 u
FORM I VOA
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FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MB030501
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.: SAS No.: SDG No.: 3MAR0501
Matrix: (soil/water) SOIL
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) G
HIGH
GC Column: RTX-502.2 ID: 0.53 (mm)
Soil Extract Volume: (mL) ----
Lab Sample ID: MB030501
Lab File ID: METIIBLKX
Date Received:
Date Analyzed: 03/05/01
Dilution Factor: 50.0
Soil Aliquot Volume: ____ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
1330-20-7-------Xylene (total) 250.0000 u
76-13-1---------Freon 113 250.0000 u
60-29-7---------Ether 250.0000 u
142-28-9--------1,3-Dichloropropane 250.0000 u
594-20-7--------2,2-Dichloropropane 250.0000 u
563-58-6--------1,1-Dichloropropene 250.0000 u
108-94-1--------Cyclohexanone 2500.0000 u
78-00-2---------Tetraethyllead 250.0000 u
141-78-6--------Ethyl acetate 250.0000 u
126-99-8--------Chloroprene 250.0000 u
FORM I VOA
FORM 2
SOIL VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.: SAS No.: SDG No.: 3MAR0501
Level: (low/med) LOW
page 1 of 1
CLIENT SMCl SMC2 SMC3 OTHER TOT
SAMPLE NO. (DCE) # (TOL)# (BFB)#
------------====== ====== :;;;;;;;;;;:;:;;;;;:::;
BLK030501 81 83 83 01
02
03
04
05
06
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08
09
10
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14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
BLK030501LCS 81 84 84
BLK030501LCS 75 82 84
MB030501
SMCl
SMC2
SMC3
(DCE)
(TOL)
(BFB)
78 85 84
QC
l,2-Dichloroethane-d4
Toluene-dB
Bromofluorobenzene
OUT
:;;;;;=::::== ---
0
0
0
0
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
LIMITS
(70-130)
(70-130)
(70-130)
# Column to be used to flag recovery values
* Values outside of contract required QC limits
D System Monitoring Compound diluted out
FORM II VOA
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FORM 3
SOIL VOLATILE LAB CONTROL SAMPLE
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.: SAS No.: SDG No.: 3MAR0501
Matrix Spike -Sample No.: blk030501 Level: (low/med) LOW
SPIKE SAMPLE LCS LCS
ADDED CONCENTRATION CONCENTRATION %
COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC #
===========--------===== -----------------------------------======
1,1-Dichloroethene 50.0000 0.0000 45.7733 92
Methylene chloride 50.0000 0.0000 46.8773 94
trans-1,2-Dichloroethen 50.0000 0.0000 48.1347 96
1,1-Dichloroethane 50.0000 0.0000 46.4665 93
Chloroform 50.0000 0.0000 46.4673 93
1,1,1-Trichloroethane 50.0000 0.0000 47.5855 95
Carbon tetrachloride 50.0000 0.0000 48.6192 97
1,2-Dichloroethane 50.0000 3.5463 47.7323 88
Benzene 50.0000 0.0000 47.2760 94
Trichloroethene 50.0000 0.0000 49.3829 99
1,2-Dichloropropane 50.0000 0.0000 46.4277 93
Bromodichloromethane 50.0000 0.0000 46.9984 94
cis-1,3-Dichloropropene 50.0000 0.0000 48.0994 96
Toluene 50.0000 0.0000 49.0761 98
trans-1,3-Dichloroprope 50.0000 0.0000 49.7582 100
1,1,2-Trichloroethane 50.0000 0.0000 49.7884 100
Tetrachloroethene 50.0000 0.0000 51.5161 103
Dibromochloromethane 50.0000 0.0000 49.6519 99
Chlorobenzene 50.0000 0.0000 50.1593 100
Ethylbenzene 50.0000 0.0000 53.2261 106
Bromoform 50.0000 0.0000 49.6689 99
1,1,2,2-Tetrachloroetha 50.0000 0.0000 45.1752 90
1,3-Dichlorobenzene 50.0000 0.0000 49.7231 99
1,4-Dichlorobenzene 50.0000 .0.0000 49. 5140 99
1,2-Dichlorobenzene 50.0000 0.0000 49.7958 100
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
COMMENTS:
page 1 of 2 FORM III VOA
QC.
LIMITS
REC.
======
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
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70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
FORM 3
SOIL VOLATILE LAB CONTROL SAMPLE
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.: SAS No.: SDG No.: 3MAR0501
Matrix Spike -Sample No.: blk030501 Level: (low/med) LOW
SPIKE LCSD LCSD
ADDED CONCENTRATION % % QC LIMITS
COMPOUND (ug/Kg) (ug/Kg) REC# RPO # RPO
----------------------------------------------;;;;::;;;;;;;;;;;;;;;;; ====== ::;:;::;====
1,1-Dichloroethene 50.0000 44.9300 90 2 20
Methylene chloride 50.0000 47.4363 95 1 20
trans-1,2-Dichloroethen 50.0000 47.7174 95 1 20
1,1-Dichloroethane 50.0000 46.8578 94 1 20
Chloroform 50.0000 46.7232 93 0 20
1,1,1-Trichloroethane 50.0000 48.0180 96 1 20
Carbon tetrachloride 50.0000 48.5600 97 0 20
1,2-Dichloroethane 50.0000 49.2929 91 3 20
Benzene 50.0000 47.2849 94 0 20
Trichloroethene 50.0000 49.2030 98 1 20
1,2-Dichloropropane 50.0000 47.2512 94 1 20
Bromodichloromethane 50.0000 47.6726 95 1 20
cis-1,3-Dichloropropene 50.0000 49. 0349 98 2 20
Toluene 50.0000 48.5484 97 1 20
trans-1,3-Dichloroprope 50.0000 50.2678 100 0 20
1,1,2-Trichloroethane 50.0000 51.0052 102 2 20
Tetrachloroethene 50.0000 49.7716 100 3 20
Dibromochloromethane 50.0000 50.5986 101 2 20
Chlorobenzene 50.0000 49.5862 99 1 20
Ethylbenzene 50.0000 52.2255 104 2 20
Bromoform 50.0000 51. 0294 102 3 20
1,1,2,2-Tetrachloroetha 50.0000 46.5253 93 3 20
1,3-Dichlorobenzene 50.0000 48.2937 96 3 20
1,4-Dichlorobenzene 50.0000 47.7880 96 3 20
1,2-Dichlorobenzene 50.0000 49.3370 99 1 20
# Column to be used to flag recovery and RPO values with an asterisk
* Values outside of QC limits
RPO: O out of 25 outside limits
Spike Recovery: 0 out of 50 outside limits
COMMENTS:
page 2 of 2 FORM III VOA
REC.
======
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
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Quality Control Summary
Volatiles
Method 8260B
Trip Blank
Analysis Date: 03/05/01
Analytical Batch ID: 3MAR0501
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FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
BLK030501
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.: SAS No.: SDG No.: 3MAR0501
Matrix: (soil/water) AQUEOUS Lab Sample ID: BLK030501
Sample wt/vol: (g/mL) ML Lab File ID:
Level: (low/med) LOW Date Received:
% Moisture: not dee.
GC Column: RTX-502.2 ID: 0.53 (mm)
Date Analyzed: 03/05/01
Dilution Factor: 1.0
Soil Extract Volume: (uL) ----Soil Aliquot Volume: ____ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-71-8---------Dichlorodifluoromethane 5.0000 u
74-87-3---------Chloromethane 5.0000 u
75-01-4---------Vinyl chloride 2.0000 u
74-83-9---------Bromomethane 5.0000 u
75-00-3---------Chloroethane 5.0000 u
75-69-4---------Trichlorofluoromethane 5.0000 u
107-02-8--------Acrolein 50.0000 u
75-35-4---------1,1-Dichloroethene 5.0000 u
75-09-2---------Methylene chloride 5.0000 u
107-13-1--------Acrylonitrile 50.0000 u
1634-04-4-------tert-Butyl methyl ether(MTBE 5.0000 u
156-60-5--------trans-l,2-Dichloroethene --5.0000 u
75-34-3c--------l,l-Dichloroethane 5.0000 u
78-93-3---------2-Butanone (MEK) 10.0000 u
67-66-3---------Chloroform 5.0000 u
74-97-5---------Bromochloromethane 5.0000 u
71-55-6---------1,1,l-Trichloroethane 5.0000 u
56-23-5---------Carbon tetrachloride 5.0000 u
107-06-2--------1,2-Dichloroethane 5.0000 u
71-43-2---------Benzene 5.0000 u
79-01-6---------Trichloroethene 5.0000 u
78-87-5---------1,2-Dichloropropane 5.0000 u
75-27-4---------Bromodichloromethane 5.0000 u
110-75-8--------2-Chloroethylvinyl ether 10.0000 u --10061-01-5------cis-l,3-Dichloropropene 5.0000 u
108-88-3--------Toluene 5.0000 u
10061-02-6------trans-l,3-Dichloropropene 5.0000 u
79-00-5---------1,1,2-Trichloroethane --5.0000 u
127-18-4--------Tetrachloroethene 5.0000 u
124-48-1--------Dibromochloromethane 5.0000 u
106-93-4--------1,2-Dibromoethane (EDB) 5.0000 u
108-90-7--------Chlorobenzene 5.0000 u
100-41-4--------Ethylbenzene 5.0000 u
FORM I VOA
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
BLK030501
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.:
Matrix: (soil/water) AQUEOUS
SAS No.: SDG No.: 3MAR0501
Lab Sample ID: BLK030501
Sample wt/vol: (g/mL) ML Lab File ID: BLK-1
Level: (low/med) LOW Date Received:
% Moisture: not dee.
GC Column: RTX-502.2 ID: 0.53 (mm)
Date Analyzed: 03/05/01
Dilution Factor: 1.0
Soil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-38-3--------m+p-Xylenes 5.0000 u
95-47-6---------o-Xylene 5.0000 u
75-25-2---------Bromoform 5.0000 u
79-34-5---------1,1,2,2-Tetrachloroethane 5.0000 u
541-73-1--------1,3-Dichlorobenzene --5.0000 u
106-46-7--------1,4-Dichlorobenzene 5.0000 u
95-50-1---------1,2-Dichlorobenzene 5.0000 u
91-20-3---------Naphthalene 5.0000 u
67-64-1---------Acetone 20.0000 u
75-05-8---------Acetonitrile 50.0000 u
74-88-4---------Methyl iodide 5.0000 u
107-05-1--------Allyl chloride 5.0000 u
75-15-0---------Carbon disulfide 5.0000 u
108-05-4--------Vinyl acetate 5.0000 u
107-12-0--------Propionitrile 50.0000 u
156-59-2-- - - - - --cis-1, 2-Dichloroe.thene 5.0000 u
126-98-7--------Methacrylonitrile 5.0000 u
80-62-6---------Methyl methacrylate 5.0000 u
74-95-3---------Dibromomethane 5.0000 u
108-10-1--------4-Methyl-2-pentanone 5.0000 u
97-63-2---------Ethyl methacrylate 5.0000 u
591-78-6--------2-Hexanone 10.0000 u
630-20-6--------1,l,l,2-Tetrachloroethane 5.0000 u -100-42-5--------Styrene 5.0000 u
96-18-4---------1,2,3-Trichloropropane 5.0000 u
110-57-6--------trans-l,4-Dichloro-2-butene 5.0000 u -100-44-7--------Benzyl chloride 5.0000 u
96-12-8---------1,2-Dibromo-3-chloropropane 5.0000 u
108-20-3--------Diisopropyl ether -5.0000 u
78-83-1---------Isobutyl alcohol 50.0000 u
123-91-1--------1,4-Dioxane 250.0000 u
95-63-6---------1,2,4-Trimethylbenzene 5.0000 u
108-67-8--------1,3,5-Trimethylbenzene 5.0000 u
.FORM I VOA
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FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
BLK030501
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.: SAS No.: SDG No.: 3MAR0501
Matrix: (soil/water) AQUEOUS
Sample wt/vol: (g/mL) ML
Level: (low/med) LOW
% Moisture: not dee.
GC Column: RTX-502.2 ID: 0.53 (mm)
Soil Extract Volume: (uL) ----
Lab Sample ID: BLK030501
Lab File ID: BLK-1
Date Received:
Date Analyzed: 03/05/01
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
1330-20-7-------Xylene (total) 5.0000 u
76-13-1---------Freon 113 5.0000 u
60-29-7---------Ether 5.0000 u
142-28-9--------1,3-Dichloropropane 5.0000 u
594-20-7--------2,2-Dichloropropane 5.0000 u
563-58-6--------1,l-Dichloropropene 5.0000 u
108-94-1--------Cyclohexanone 50.0000 u
78-00-2---------Tetraethyllead 5.0000 u
141-78-6--------Ethyl acetate 5.0000 u
126-99-8--------Chloroprene 5.0000 u
FORM I VOA
FORM 2
AQUEOUS VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code:
page 1 of 1
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Case No.:
CLIENT
SAMPLE NO.
_;;:;:=========
BLK030501
BLK030501LCS
BLK030501LCS
SMCl
(DCE)#
======
81
81
75
SAS No.: SDG No.: 3MAR0501
SMC2 SMC3 OTHER TOT
(TOL)# (BFB) # OUT
====== :;:::::;;;;;;: = ;;:===== ---
83 83 0
84 84 0
82 84 0
-
---
-
-
-
-
-
-
-
-
--
-
-
-
-
--
-
--
-
-
-
-
--
--
-
SMCl
SMC2
SMC3
(DCE)
(TOL)
(BFB)
QC
l,2-Dichloroethane-d4
LIMITS
(70-130)
(70-130)
(70-130)
= Toluene-dB
= Bromofluorobenzene
# Column to be used to flag recovery values
* Values outside of contract required QC limits
D System Monitoring Compound diluted out
FORM II VOA
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I FORM 3
AQUEOUS VOLATILE LAB CONTROL SAMPLE
I Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code : Case No. : SAS No. : SDG No.: 3MAR0501 I
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Matrix Spike -Sample No.: blk030501
SPIKE SAMPLE LCS LCS
ADDED CONCENTRATION CONCENTRATION %
COMPOUND (ug/L) (ug/L) (ug/L) REC #
======================== -----------------------------------======
1,1-Dichloroethene 50.0000 0.0000 45.7733 92
Methylene chloride 50.0000 0.0000 46.8773 94
trans-1,2-Dichloroethen 50.0000 0.0000 48 .1347 96
1,1-Dichloroethane 50.0000 0.0000 46.4665 93
Chloroform 50.0000 0.0000 46.4673 93
1,1,1-Trichloroethane 50.0000 0.0000 47.5855 95
Carbon tetrachloride 50.0000 0.0000 48.6192 97
1,2-Dichloroethane 50.0000 0.0000 47.7323 95
Benzene 50.0000 0.0000 47.2760 94
Trichloroethene 50.0000 0.0000 49.3829 99
1,2-Dichloropropane 50.0000 0.0000 46.4277 93
Bromodichloromethane 50.0000 0.0000 46.9984 94
cis-1,3-Dichloropropene 50.0000 0.0000 48.0994 96
Toluene 50.0000 0.0000 49.0761 98
trans-1,3-Dichloroprope 50.0000 0.0000 49.7582 100
1,1,i-Trichloroethane 50.0000 0.0000 49.7884 100
Tetrachloroethene 50.0000 0.0000 51. 5161 103
Dibromochloromethane 50.0000 0.0000 49.6519 99
Chlorobenzene 50.0000 0.0000 50.1593 100
Ethyl benzene 50.0000 0.0000 53.2261 106
Bromoform 50.0000 0.0000 49.6689 99
1,1,2,2-Tetrachloroetha 50.0000 0.0000 45.1752 90
1,3-Dichlorobenzene 50.0000 0.0000 49.7231 99
1,4-Dichlorobenzene 50.0000 0.0000 49. 5140 99
1,2-Dichlorobenzene 50.0000 0.0000 49.7958 100
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
COMMENTS:
page 1 of 2 FORM III VOA
QC.
LIMITS
REC.
=====:::
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
FORM 3
AQUEOUS VOLATILE LAB CONTROL SAMPLE
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code : Case No . : SAS No . : SDG No.: 3MAR0501
Matrix Spike -Sample No.: blk030501
SPIKE LCSD LCSD
ADDED CONCENTRATION % % QC LIMITS
COMPOUND (ug/L) (ug/L) REC# RPD # RPD REC.
----------------------------------------------====:;:::= :;;:;:::==== ====== ======
1,1-Dichloroethene 50.0000 44.9300 90 2 20 70-13 0
Methylene chloride 50.0000 47.4363 95 1 20 70-13 0
trans-1,2-Dichloroethen 50.0000 47.7174 95 1 20 70-13 0
1,1-Dichloroethane 50.0000 46.8578 94 1 20 70-130
Chloroform 50.0000 46.7232 93 0 20 70-13 0
1,1,1-Trichloroethane 50.0000 48.0180 96 1 20 70-130
Carbon tetrachloride 50.0000 48.5600 97 0 20 70-130
1,2-Dichloroethane 50.0000 49.2929 98 3 20 70-130
Benzene 50.0000 47.2849 94 0 20 70-130
Trichloroethene 50.0000 49.2030 98 1 20 70-130
1,2-Dichloropropane 50.0000 47.2512 94 1 20 70-130
Bromodichloromethane 50.0000 47.6726 95 1 20 70-130
cis-1,3-Dichloropropene 50.0000 49.0349 98 2 20 70-130
Toluene 50.0000 48.5484 97 1 20 70-130
trans-1,3-Dichloroprope 50.0000 50.2678 100 0 20 70-130
1,1,2-Trichloroethane 50.0000 51. 0052 102 2 20 70-130
Tetrachloroethene 50.0000 49.7716 100 3 20 70-130
Dibromochloromethane 50.0000 50.5986 101 2 20 70-130
Chlorobenzene 50.0000 49.5862 99 1 20 70-130
Ethyl benzene 50.0000 52.2255 104 2 20 70-130
Bromoform 50.0000 51.0294 102 3 20 70-13 0
1,1,2,2-Tetrachloroetha 50.0000 46.5253 93 3 20 70-130
1,3-Dichlorobenzene 50.0000 48.2937 96 3 20 70-130
1,4-Dichlorobenzene 50.0000 47.7880 96 3 20 70-130
1,2-Dichlorobenzene 50.0000 49.3370 99 1 20 70-13 0
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: O out of 25 outside limits
Spike Recovery: 0 out of 50 outside limits
COMMENTS:
page 2 of 2 FORM III VOA
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I Quality Control Summary
I Semivolatiles
Method 8270C
I
I Extraction Date: 03/02/01
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FORM 1 CLIENT SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MB2227
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.:
Matrix: (soil/water) SOIL
SAS No.: SDG No.: 7MAR0201
Lab Sample ID: 2227MB
Sample wt/vol:
Level: (low/med)
30.0 (g/mL) G
LOW
Lab File ID: 0302A20
Date Received:
% Moisture: 0 decanted: (Y/N) N
Concentrated Extract Volume: 5000 (uL)
Injection Volume: ___ (uL)
Date Extracted:03/02/01
Date Analyzed: 03/02/01
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
62-75-9---------N-Nitrosodimethylamine
lll-44-4--------bis(2-Chloroethyl)ether
108-95-2--------Phenol
95-57-8---------2-Chlorophenol
106-46-7--------1,4-Dichlorobenzene
541-73-1--------1,3-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
108-60-l--------bis(2-Chloroisopropyl)ether
621-64-7--------n-Nitroso-di-n-propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophen6I
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-82-1--------1,2,4-Trichlorobenzene -
120-83-2--------2,4-Dichlorophenol
91-20-3---------Naphthalene
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
88-06-2---------2,4,6-Trichlorophenol
91-58-7---------2-Chloronaphthalene
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
83-32-9---------Acenaphthene
121-14-2--------2,4-Dinitrotoluene
86-73-7---------Fluorene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenylphenylether
86-30-6---------n-Nitrosodiphenylamine_(l/
101-55-3--------4-Bromophenylphenylether __
118-74-1--------Hexachlorobenzene
' ' (1) -Cannot be separated from D1phenylam1ne
FORM I SV
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
333.3333
Q
u
u
u
u
u
u u
u
u
u u
u
u
u u
u
u
u u
u
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u u
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FORM 1 CLIENT SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MB2227
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.:
Matrix: (soil/water) SOIL
SAS No.: SDG No.: 7MAR0201
Lab Sample ID: 2227MB
Sample wt/vol:
Level: (low/med)
30.0 (g/mL) G
LOW
Lab File ID: 0302A20
Date Received:
% Moisture: 0 decanted: (Y/N) N
Concentrated Extract Volume: 5000 (uL)
Injection Volume: (uL)
Date Extracted:03/02/01
Date Analyzed: 03/02/01
Dilution Factor: 1.0 ----
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
85-01-8---------Phenanthrene 333.3333
120-12-7--------Anthracene 333.3333
84-74-2---------Di-n-butylphthalate 333.3333
206-44-0--------Fluoranthene 333.3333
92-87-5---------Benzidine 833.3333
129-00-0--------Pyrene 333.3333
85-68-7---------Butylbenzylphthalate 333.3333
56-55-3---------Benzo(a)Anthracene 333.3333
91-94-1---------3,3'-Dichlorobenzidine 333.3333
218-01-9--------Chrysene 333.3333
117-81-7--------bis(2-Ethylhexyl)phthalate_ 333.3333
117-84-0--------Di-n-octylphthalate 333.3333
50-32-8---------Benzo(a)pyrene 333.3333
193-39-5--------Indeno(l,2,3-c,d)pyrene 333.3333
53-70-3---------Dibenzo(a,h)anthracene 333.3333
191-24-2--------Benzo(g,h,i)perylene 333.3333
534-52-1--------4,6-Dinitro-2-methylphenol_ 833.3333
87-86-5---------Pentachlorophenol 833.3333
95-48-7---------o-Cresol 333.3333
106-44-5--------m+p-Cresol 333.3333
106-47-8--------4-Chloroaniline 333.3333
91-57-6---------2-Methylnaphthalene 333.3333
95-95-4---------2,4,5-Trichlorophenol 333.3333
90-13-1---------1-Chloronaphthalene 333.3333
88-74-4---------2-Nitroaniline 333.3333
99-09 0 2---------3-Nitroaniline 333.3333
132-64-9--------Dibenzofuran 333.3333
100-01-6--------4-Nitroaniline 333.3333
122-39-4--------Diphenylamine 333.3333
91-80-5---------Methaphyrilene 833.3333
77-47-4---------Hexachlorocyclopentadiene 833.3333
51-28-5---------2,4-Dinitrophenol --833.3333
103-33-3--------Azobenzene 333.3333
FORM I SV
Q
u u u
u
u u u u
u
u
u
u
u
u u
u
u
u
u u u
u
u
u u
u
u u u
u
u
u
u
FORM 1 CLIENT SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol:
Level: (low/med)
% Moisture: 0
30.0 (g/mL) G
LOW
decanted: (Y/N) N
SAS No.:
Concentrated Extract Volume: 5000 (uL)
Injection Volume: (uL) ----
GPC Cleanup: (Y/N) N pH: 7.0
MB2227
SDG No.: 7MAR0201
Lab Sample ID: 2227MB
Lab File ID: 0302A20
Date Received:
Date Extracted:03/02/01
Date Analyzed: 03/02/01
Dilution Factor: 1.0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
100-02-7--------4-Nitrophenol 833.3333 u
119-93-7--------3,3'-Dimethylbenzidine 833.3333 u
65-85-0---------Benzoic acid 8333.3333 u
134-62-3--------Deet 333.3333 u
51-03-6---------Pip 833.3333 u
86-748----------Carbazole 333.3333 u
205-99-2--------Benzo(b)fluoranthene 333.3333 u
207-08-9--------Benzo(k)fluoranthene 333.3333 u
100-51-6-- ---- --Benzyl _Alcohol 333.3333 u
FORM I SV
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FORM 1 CLIENT SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: SHEALY ENVIRONMENTAL SERV
Lab Code: Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol:
Level: (low/med)
30.0 (g/mL) G
LOW
MB2227
Contract:
SAS No.: SD3 No.: 4MAR0301
Lab Sample ID: 2227MB
Lab File ID: 0303A03
Date Received:
% Moisture: 0 decanted: (Y/N) N Date Extracted:03/02/01
Date Analyzed: 03/03/01
Dilution Factor: 1.0
Concentrated Extract Volume: 5000 (uL)
Injection Volume: ___ (uL)
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
101-84-8--------Phenyl ether
92-52-4---------Biphenyl
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
333.3333
333.3333
FORM I SV
Q
u
u
FORM 2
SOIL SEMIVOLATILE SURROGATE RECOVERY
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.: SAS No.: SDG No.: 7MAR0201
Level: (low/med) LOW
CLIENT Sl S2 S3 S4 S5 S6 S7
SAMPLE NO. (2FP) # (PHL)# (NBZ)# (FBP)# (TBP)# (TPH)# #
------------;;;;;;:=:;::;::;::;; =:===== ====== ====== =;:;;:;::;::;:;;:;;; ;;:===== ======
01
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MB2227
MB2227LCS
page 1 of 1
71 67 63 64 50 89
75 70 67 69 69 87
.
.
QC LIMITS
Sl (2FP) 2-Fluorophenol (30-130)
S2 (PHL) = Phenol-d5 (30-130)
SJ (NBZ) Nitrobenzene-d5 (30-130)
S4 (FBP) = 2-Fluorobiphenyl (30-130)
S5 (TBP) = 2,4,6-Tribromophenol (30-130)
S6 (TPH) Terphenyl-dl4 (30-130)
# Column to be used to flag recovery values
* Values outside of contract required QC limits
D Surrogate diluted out
FORM II SV
SB
#
======
TOT
OUT
---
0
0
-
-
-
-
-
-
-
--
-
-
--
-
-
-
-
-
---
-
-
--
-
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-
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FORM 3
SOIL SEMIVOLATILE LAB CONTROL SAMPLE
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No. : SAS No.: SDG No.: 7MAR0201
Matrix Spike -Sample No. : mb2227 Level: (low/med) LOW
SPIKE SAMPLE LCS LCS
ADDED AMOUNT AMOUNT %
COMPOUND (ug/mL) (ug/mL) (ug/mL) REC #
-----------------------------------------------------------;;;;;;;;;;;;
Phenol 20.0000 0.0000 14.6227 73
2-Chlorophenol 20.0000 0.0000 14.4708 72
1,4-Dichlorobenzene 20.0000 0.0000 12.6354 63
n-Nitroso-di-n-prop. (1) 20.0000 0.0000 13.6933 68
1,2,4-Trichlorobenzene 20.0000 0.0000 13. 6289 68
4-Chloro-3-methylphenol 20.0000 0.0000 14.2806 71
Acenaphthene 20.0000 0.0000 13. 8894 69
2,4-Dinitrotoluene 20.0000 0.0000 10.9655 55
Pyrene 20.0000 0.0000 19.5949 98
Pentachlorophenol 20.0000 0.0000 12. 9114 64
4-Nitrophenol 20.0000 0.0000 9.1786 46
(1) N-Nitroso-di-n-propylamine
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: 0 out of O outside limits
Spike Recovery: 0 out of 11 outside limits
COMMENTS:
FORM III SV
QC.
LIMITS
REC.
;::;:;;;;;;:;;;;:::::
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
10-130
FORM 3
SOIL SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.: SAS No.: SDG No.: 7MAR0201
Matrix Spike -Sample No.: cc02001-001 Level: (low/med) LOW
SPIKE SAMPLE MS MS QC.
ADDED AMOUNT AMOUNT % LIMITS
COMPOUND (ug/mL) (ug/mL) (ug/mL) REC # REC.
======================== -----------------------------------====== :=c=====
Phenol 20.0000 0.0000 7.3137 36 30-130
2-Chlorophenol 20.0000 0.0000 7.1947 36 30-130
1,4-Dichlorobenzene 20.0000 0.0000 6.4000 32 30-130
n-Nitroso-di-n-prop. (1) 20.0000 0.0000 6.8909 34 30-130
1,2,4-Trichlorobenzene 20.0000 0.0000 6.7107 34 30-130
4-Chloro-3-methylphenol 20.0000 0.0000 7.4036 37 30-130
Acenaphthene 20.0000 0.0000 7 .1137 36 30-130
2,4-Dinitrotoluene 20.0000 0.0000 7.1821 36 30-130
Pyrene 20.0000 0.0000 10.4144 52 30-130
Pentachlorophenol 20.0000 0.0000 9.0017 45 30-130
4-Nitrophenol 20.0000 0.0000 6.2266 31 10-130
SPIKE MSD MSD
ADDED AMOUNT % % QC LIMITS
COMPOUND (ug/mL) (ug/mL) REC # RPD # RPD
----------------------------------------------====== ====== :::;;:;;:::::::::
Phenol 20.0000 15.2856 76 71* 40
2-Chlorophenol 20.0000 15.2610 76 71* 40
1,4-Dichlorobenzene 20.0000 13.2403 66 69* 40
n-Nitroso-di-n-prop. (1) 20.0000 14.2886 71 70* 20
1,2,4-Trichlorobenzene 20.0000 13.6831 68 67* 40
4-Chloro-3-methylphenol 20.0000 15.3596 77 70* 40
Acenaphthene 20.0000 14.6619 73 68* 40
2,4-Dinitrotoluene 20.0000 15.3073 76 71* 40
Pyrene 20.0000 19.3204 97 60* 40
Pentachlorophenol 20.0000 14.5416 73 47* 40
4-Nitrophenol 20.0000 12.8341 64 69* 40
(1) N-Nitroso-di-n-propylamine
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: 11 out of 11 outside limits
Spike Recovery: 0 out of 22 outside limits
COMMENTS:
FORM III SV
REC.
======
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
30-130
10-130
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I Quality Control Summary
Methanol
I Method 8015B
I Analyzed: 03/05/01
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FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MB030401
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: (g/mL) G
Level: (low/med)
% Moisture: not dee.
GC Column: RTX-5
LOW
ID: 0.32 (mm)
Soil Extract Volume: (mL) ---
CAS NO. COMPOUND
67-56-1---------Methanol
SAS No.: SDG No.: 030501Sl
Lab Sample ID: MB030401
Lab File ID: 01881801
Date Received:
Date Analyzed: 03/05/01
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL)
CONCENTRATION UNITS:
(ug/L or ug/Kg) MG/KG Q
----------1.ool_u __
FORM I VOA
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FORM 3
SOIL VOLATILE LAB CONTROL SAMPLE
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code : Case No . : SAS No.: SDG No.: 030501Sl
Matrix Spike -Sample No.: mb030401 Level: (low/med) LOW
SPIKE SAMPLE LCS LCS
ADDED AMOUNT AMOUNT %
COMPOUND (ug/mL) (ug/mL) (ug/mL) REC #
-----------------------------------------------------------======
Methanol 500.00 0.00 526.68 105
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: 0 out of O outside limits
Spike Recovery: 0 out of 1 outside limits
COMMENTS:
FORM III VOA
QC.
LIMITS
REC.
======
50-130
FORM 3
SOIL VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.: SAS No.: SOO No.: 030501Sl
Matrix Spike -Sample No.: cc02001-007 Level: (low/med) WW
SPIKE SAMPLE MS MS QC.
ADDED AMOUNT AMOUNT % LIMITS
COMPOUND (ug/mL) (ug/mL) (ug/mL) REC # REC.
======================== -----------------------------------:::::::::::=:;::= ===;::;::;:=:
Methanol 500.00 0.00 530.92 106 50-130
SPIKE MSD MSD
ADDED AMOUNT % % QC LIMITS
COMPOUND (ug/mL) (ug/mL) REC # RPD # RPD
---------------------------------============= :::::::::::;:;;;;:::; ::::;:::==== ======
Methanol 500.00 491.99 98 8 40
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: O out of 1 outside limits
Spike Recovery: 0 out of 2 outside limits
COMMENTS:
FORM III VOA
REC.
======
50-130
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Quality Control Summary
Ethylene Glycol & Diethylene Glycol
Method 8015B
Analyzed: 03/02/01
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MB030201
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.: SAS No.: SDG No.: 030201Sl
Matrix: (soil/water) SOIL
Sample wt/vol: (g/mL) G
Level: (low/med)
% Moisture: 0
LOW
decanted:
Concentrated Extract Volume:
Injection Volume: ___ (uL)
GPC Cleanup: (Y/N) N
(Y/N) N
5 (mL)
pH: 7.0
CAS NO. COMPOUND
Lab Sample ID: MB030201
Lab File ID: 018B1701
Date Received:
Date Extracted:03/02/01
Date Analyzed: 03/02/01
Dilution Factor: 1.0
CONCENTRATION UNITS:
(ug/L or ug/Kg) MG/KG
50.00
Q
u 107-21-1--------Ethylene Glycol
111-46-6--------Di(ethylene glycol) 50.00 u
FORM I VOA
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FORM 3
SOIL VOLATILE LAB CONTROL SAMPLE
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code : Case No . : SAS No.: SDG No.: 03020181
Matrix Spike -Sample No.: mb030201 Level: (low/med) LOW
SPIKE SAMPLE LCS LCS
ADDED AMOUNT AMOUNT %
COMPOUND (ug/mL) (ug/mL) (ug/mL) REC #
======================== -----------------------------------:;;;;:;;:;:;;;::;:;::;:;;;
Ethylene Glycol 500.00 0.00 432.10 86
Di(ethylene glycol) 500.00 0.00 437.73 88
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: 0 out of O outside limits
Spike Recovery: 0 out of 2 outside limits
COMMENTS:
FORM III VOA
QC.
LIMITS
REC.
======
50-130
50-130
FORM 3
SOIL VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: SHEALY ENVIRONMENTAL SERV Contract:
Lab Code: Case No.: SAS No.: SDG No.: 030201Sl
Matrix Spike -Sample No.: cc02001-008 Level: (low/med) LOW
SPIKE SAMPLE MS MS QC.
ADDED AMOUNT AMOUNT % LIMITS
COMPOUND (ug/mL) (ug/mL) (ug/mL) REC # REC.
======================== -----------------------------------====== =====;:
Ethylene Glycol 500.00 0.00 87.72 18* 50-130
Di(ethylene glycol) 500.00 0.00 44.81 9 50-130
SPIKE MSD MSD
ADDED AMOUNT % % QC LIMITS
COMPOUND (ug/mL) (ug/mL) REC # RPD # RPD
----------------------------------------------====== ;::;:;:::::=== ======
Ethylene Glycol 500.00 375.90 75 122* 40
Di(ethylene glycol) 500.00 308.24 62 149* 40
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: 2 out of 2 outside limits
Spike Recovery: 1 out of 4 outside limits
COMMENTS:
FORM III VOA
REC.
======
50-130
50-130
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Quality Control Summary
Acetic Acid
Method 300.0
(Subcontracted)
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03-05-2001 IO: 12am From-111:TROHM-PEAK 281-648-5551 T-489 P.001/001 F-927
Metrohm-Peak Inc.
Shea.l,y Environmental Services
· Lab Renort 201-1_202
March ~. 2001
I ·-
I
Sample I Acetic .-I ma/Ka --
~-I ..
cco2001-001 I nd ..
CC02001-001 D~e-nd
Mean --
CC02001-002 I 539.293
cco2001.003 I nd
CC02001-004 1403.322
CC02001-005 1496.643
CC02001-006 121~.760 --CC02001-007 ~
cco2001-ooa nd -! QC 9.631
QC Value 10.000
% Recover}'. 96.310
I ·-
Sx Detection Limit 0.300
USE BALL POINT PEN ONLY, PRESS HARD
CHAIN OF CUSTODY #
Client Name \(.L{ G1[-n\ f l'L--
Reporting Addres•~ F Q, 'Yl/)-,( fJD Z<../.-7 < , wP ~uJ vi t l t 5 c.-
Attention :5 /M -\-'U (l.d...--,
Telephone No. C/sb</,~q(;, 7~q(/P'1rJ' No2b"1lbl
Sample ID (Location) v,£J-~ 0 0 "' TIME u:l ::::; , ;l' DAT ~ g 8 "
Star1 Of5b t y5 F1msh
Al1f-l)L-14
Stan f{} 3o
K I ..,
F,n,sh ' C)
S1ar1 ( l'.OC
F,msh ,. / . '. ..,
Stan
Fm1sh
Stan
Ftn1sh IX
Stan
fccFio-,,o---+-{)~: 1_0 ~ ~ ':)
Star1
Fm,sh
Relinquished by (Sig.)
.
Relinqui~g~ A I Date/Timp. )\1 J h, I (')'~ :,Q - -
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Pointe Drive
Cayce, South Carolina 29033
Telephone No. [phone] Fax No. [phone]
L ·2--Page ot_
NPDES# __________ _
County ___________ _
CHAIN OF CUSTODY RECORD Receiving Stream ________ _
SAMPLE ANALYSIS REQUIRED
i €
~ ~ ~ 0 00 <!'¥ ~ 00 ' i ' X i~ 00 0 h ~ ~8 " 0 ~ c X
ci g w 8f 0 w ~ 0 "' z• , ~ "' >>
'X
y
/...
X.
X
X
X
Date/Time
Received by (Sig.) Date/Time
I
-
Outfall No. __________ _
.. PRESERVATION (CODE)
CODE: A= None
B = HNO3
C = H2S04
D = NaOH
E = ICE
F-
REMARKS
SVOC -'62--=f O
M (~c.. Soi v cvY(.;
C.wf A~-nc.... h-t;&--
~e..e.__ ta: s It--
Hazards Associated with Sample
-- - -
LAB USE ONLY
Program Area (Circle)
DW CWAINPDES
ACRA SPISOL
SP/LIQ Other: __
SESI
LABI.D.
C ('_ n ,'.:)on I "'1
Cb3
ON
cxfo
Cus1ody Seal Intact (Cirde)
YES NO NONE
Roceip! TAC ___ mg/1
Receipt pH•--~-'"
R,1 " Roce~ Terrp .
_Xeived on_ Ice (Cirde)
/_YE) NO ICE PACK
--CHAIN OF GUST~ # r-;-
Client Name {l.t... f--ll, l Q_ 'f2._
P7) uX gD~7 Reporting Address s / fr/ PS&J V\ l',/t--~ c.. Z"S6.G'o
Attention .::::S I -"' HJV.1---
Telephone No ...... ---9-;pL J'J&z-W--, PON2{;,M/~/
,
y~~ J 0 ~ m Sample ID (Location) TIME J :; , ~ ~ 0 0 00 L) " S•:;__r ( -X 12 tlll~ WL Fm1sh
1--'
Start
) Finish
( Start
F,msh
) Start
F,msh
I Start
Fmish
( Start
F1msh
Start
F,msh
Start
Finish
SAMPLER~ jf\ fu e,t'._.-~Ir:;•~#:: Print Name\
~ ~ Signature_;....;'\ '--.....\
Relinquish~ (Sig.) Date/Time
I
Relinquish~'.~.[ t _ -u v-Z, f J,tץ;,im~ J3t\
1 White Copy: SamplM I
-4-1 IVI_M.,_.L ~IC-Na.II
106 Vantage Pointe Drive
Cayce, South Carolina 29033
Telephone No. [phone] Fax No. [phone]
CHAIN OF CUSTODY RECORD
SAMPLE ANALYSIS REQUIRED
~
~ i )i_ t t ~ ,-0 00 ?¥ l ~ 00 ' 00
~ ' X ~g 00 ' C ~ 0 ' • ~ 0 It ~ ~8 . 0 E L) 0 < X ~ 0 a ' c; a is w 8f i& ci 0 w a z ~ u I"-0 m rn , a m >> m us
- -- -NPDES# _____________ _
County _____________ _
Receiving Stream __________ _
0 !fall N u o.
+-PRESERVATION (COOEJ LAB USE ONLY
CODE: A. None Program Area (Circle) Ba HNO3 DW CWAINPDES C. H2S04 RCRA SP/SOL D • NaOH SP/LIQ Other· Ea ICE --
F•
SESI REMARKS LAB I.D.
~ ~7--66 odl
(J
Received by (Sig.) Date/Time Hazards Associated with Sample CustOdy Seat Intact (Citde)
) YES NO NONE
ftbzy :?:J, lb/ 17: 3b Receipt TAC ""'
Recept pH 9 '" Received by (Sig.) Date/Time § I Rece~ Te~. -c
~~tcr?1~';t j_ -~ 3h1t"t7!tJ6 ~tved on Ice (Cirde)
NO ICE PACK -j VVellow Copy: SheatY Pl'rwt--Copy: Report
Sample Receipt Checklist
Cooler received by/date: /Cf vUVt i '3 2-01 Lot number: C c«rzoo I
Means of receipt: 0 SES! □ Client 0 UPS [}-FedEx 0 DirectX 0 Other
Cooler temperature upon receipt ,;>.C/ oc
Method: □ Temperature Blank E:f'Against Bottles
Method of coolant: r:;}-'wet Ice
/ □ Blue Ice □ Dry Ice □ None
Yes / No □ NA □ I. Is the shinner's packing slip attached to this form? (if aop)icable)
Yes , --No □ NA □ 2. Was a chain of custody provided with the samples?
Yes / -No NA □ 3. Were proper custody procedures followed? --
Yes / _No □ NA □ 4. Was the client name listed?
Yes / --No NA □ 5. Were sample IDs listed?
Yes / _No NA □ 6. Was collection date & time listed?
Yes / -No □ NA □ 7. Were the tests to be performed listed on either the C of C or quote?
Yes , No I NA □ 8. Did all samples arrive in the proper containers for each test?
Yes V No □ NA □ 9. Did all bottle labels aPTee with custody papers?
Yes / No □ NA □ 10. Did all containers arrive in good condition (unbroken)?
Yes / No NA 11. Was adequate samole volume available?
Yes 0 No □ NA □ 12. Were all samples received within ½ the holding time or 48 hours, whichever
comes first?
Yes No , -NA □ 13. Were any samples containers missing?
Yes No I/ -NA □ 14. Were there any excess samples not listed on C ofC?
Yes □ No □ NA --15. Were air bubbles >6 mm in any VOA vials (if aoolicable)?
Yes □ No □ NA / 16. Were all Metals; Oil & Grease; Nutrient samp\es received at a pH of <2? /
Yes I I No I NA ,-17. Were all Cvanide; Sulfide samples received at a pH >12?
Yes □ No □ NAg---, 18. Were all NH3; TKN; Cyanide; BNA; PEST; PCB; HERB samples free of
residual chlorine?(< 0.2 mg/L)
Yes □ No □ NAE] 19. For North Carolina samples, were collection temperatures documented on
the chain of custody?
Sample Preservation (Must be completed for any sample(s) incorrectly preserved.)
Sample(s) were received incorrectly preserved and were
adiusted accordingly in sample receiving.
Sample(s) were received incorrectly preserved and were
unable to be analyzed.
Sample(s) were received with bubble >6 mm in diameter
Corrective Action taken, if necessary:
Wasclientnotified: Yes o Non PRIOR\1V OVERNIGH1
Did client respond: Yes O l ~ -Deliver By,
Date of response: enp• 99519 0•1MAROl 02MAR~\
Shealy employee: ----1RK• 8166 9016 3584 ~~~~ CAE Cli'f€b'ACEk~ 29033 -sc-us 28 USCA
FRI
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Grab Sampling Log-Soil
Project No. ;;i. lQ Mr o , Site Location: CN Pc --~h.e, lb'-1 b\C I I
Sample Date: sl l Loi Anival Time: oq: so Sample Time: 09~50 r,
Sample ID: t::DJ?-G .;).-7 Duplicate: Y/0 Field Personnel: ~LTF I
Sample Depth: 7 ft Weather:
Description of Lithology: C~o..y ,G' I \ 1 Cc d d-r, be()<...;-)(\ 1 ()O cQoc
Sampling Method: H:a cfl Q '"tJ c:-r
Method(s) Container Desription Preser....ative
voe s Voes l x -4 o:z.
I ,I( 9oz
Remarks: ------------------------
Sample Date: 3 J 1./ 61 r I
Sample ID NTf=" -6i,-\it
Sample DeJ)th: \ 4-tt
Arrival Time ()9' '. 30
Duplicate: Y , 8
Sample Time I /) : 3 0
Field Personnel: StJ / Jt= i
Weather: ----
'
Description of Lithology C \ a..y ::h I( I eccl ::h, b0:/1>-lD J s:+aiqs cdo-.
Sampling Method: H-o,:..d Q. 1-1.3:c: C
Method(s) Container Desriplion Preservative
/ M ';, <.r . ,
Remarks: _______________________ _
•
Kubal-Furr Associates Revi~d 2.5.99
Grab Sampling Log-Soil
Project No. J ~ W\I O\ Site Location: C NA -Shel-lay I NC
Sample Date: 3 } J / O I . Anival Time:
J I
/ 0 ·. SS:: Sample Time: \ I : 00
Sample ID: filp -01 -;;i Duplicate: y ,Gi') Field Personnel: ~N ,6:-F
Sample Depth: (;i tt Weather: ___ _
Description or Lithology: C\ o. y: £'II I red ::-\e \:)(7>, '-'><"> ) nc, od o,
Sampling Method: b:\:a,ndl 0, 't'JC C
Method(s)
'I/cc C,
Yoe.,
Container Desription
3 x 4-0 v-.-.L \[ 0 Pr
\ Y 4-0:z-
I •X '10z_.. '
Preservative
-
Remarl<s: ________________________ _
Sample Date: < j I ,l O I Arrival Time: 10·.s:S:-Sample Time: 11·.4s T I
Sample ID: }'\TP-Cll-lS Duplicate: Y/Gi) Field Personnel: St--:1 L~ i
Sample De~th: I -=>.i tt Weather:
i
Description or Lithology: C,\o_y f;\ l 1 1( d =:k, b~,::,X\ ) ;:,:\-D:zQ& cdo r
Sampling Method: 't\e,, 0d 0-.03 c.,
Method(s) Container Desriplion Preservative
----
Remarks: ________________________ _
•
Kubal-Furr Associates Revis.ad 2.5.99
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Grab Sampling Log-Soil
Project No. ,;)le ~0\ Site Location: ..,,C-'.N'-=-'Pc'-'---_-_-:....~'.:>.,_,h'---'-"'-c _,__1-""b'--'ly'-ll-lfJ~C~
Sample Date: 7/1 /01 r 1
Arrival Time: J ~ ·. ( S
Sample ID: NIE --o.3 --s Duplicate: v ,(t[)
Sample Time: ) 3 '. 3 O
Field Personnel: SN /"JF I
Sample Depth: s: tt VVeather: ___ _
Desaiption or Lithology: C\ c,,,y :ti\\ I o-:d :::k, bn,c._,0 ) oo cdev '
i
Sampling Method: \-:-\--<:\xx;! Q,,,\,~ S::C
Method(s) Container Desriplion Preservative
Remarks: ________________________ _
Sample Date: 3 /1 } 6 ( Arrival Time: J 3'. ;-j S"" I ;
Sample ID: NTE---03 -13 Duplicate v ,G)
Sample Time: l-4 :oc;;
Field Personnel: ,SN /JP
'
Sample Dei]th: 16 tt Weather: ___ _
Desaiption or Lithology: C\ 0-.f B \ I ' ced :±, b@<.)-..)0 ) s:\:@05 odor
Sampling Method: _,_fb--\-(r::1,;.r:a"'c--4\ _ _,~"""u"-'6'\-''-·-'-r-________________ _
Method(s) Container Desription Preservative
V
Svoc~ -
Remarks: ________________________ _
•
Kubal-Furr Associates Revisad 2.5.99
Grab Sampling Log-Soil
Project No. dlo MI.GI Site Location: ( N f?.;. --Sh<-\ by , NC
Sample Date: ~L1 /01 Arrival Time: I 4: ,)& Sample Time: is· 10
1 ' Sample ID: t-JTJ=--04-13 Duplicate: y ,(ii') Field Personnel: SN l~ •
Sample Depth: 13 ft Weather:
Desaiptionoflithology: C\o..'/ £11 Ired+, h[{}c,0<\ 100 co/o,'
'
Sampling Method: \Je,\:11 ci, L:Y" c
Method(s) Container Desription Preservative
3 >< 4o,,,., L \/~-A;
Remarks: ------------------------
Sample Date: 3 I , .J o 1 r • Arrival Time: Sample Time / \,, : 0'5 15·.3o
Sample ID: f':-JTE-OS-8 Duplicate: Y W Field Personnel: 3'J / J"F ----'--'-"---''-----.
Sample DeJ)th: 'd ft Weather: ___ _
Description of Lithology: c, °'Y tl 11 : ce.d --½ b{o WC, l ao ado,
Sampling Method: l:bi.,lo(';I g ~"-':C
Method(s) Container Desriplion Preservative
VDC.s
Remarks: _______________________ _
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Kubal-Furr Associates Re..,;s-ad 2.5.99
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