NCD003446721_20000313_Celeanse Corporation - Shelby Fiber_FRBCERCLA RA_OU-1 Semiannual Report July - December 1999-OCR

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Operable Unit 1-Semiannual Report
July 1999-December 1999
CNA Holdings, Inc.
Shelby, North Carolina
(F.K.A. Hoechst Celanese Corporation)
Document Control No. 026S8-0087
Submitted to,
U.S. Environmental Protection Agency
Region IV
Atlanta, Georgia
Prepared for
CNA Holdings, Inc.
Shelby, North Carolina
March 2000
Kubal-Furr & Associates
RECEIVED
MAR 14 2000
SUPERFUND SECTION
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Post Office Box 273210
Tampa, FL 33688-3210
[phone]
FAX [phone]
[e-mail]
Mr. McKenzie Mallary
Remedial Project Manager
U.S. Environmental Protection
Agency, Region IV
100 Alabama St., S.W.
Atlanta, GA 30303-3014
Dear Ken:
Kubal-Furr & Associates
Environmental Management Services
March 13, 2000
Post Office Box 80247
Simpsonville, SC 29680-0247
[phone]
FAX [phone]
[e-mail]
On behalf of CNA Holdings, Inc., we are pleased to enclose two copies of the report entitled:
"Operable Unit I-Semiannual Report-July 1999-December 1999-CNA Holdings,
Inc.-Shelby, North Carolina." By way of this letter, we have also transmitted a copy of the
report to Bruce Nicholson with NCDENR for his review.
Please get back with either Mr. Jerry McMurray at 704-480-4656, or me, to discuss any
questions you may have following your review of this document.
Sincerely,
Kubal-Furr & Associates
J:!:~~ Presi$-n~ub
cc: Mr. Bruce Nicholson, NCDENR
Mr. Jerry McMurray, Ticona-Shelby ESHA
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Contents
Page
Introduction ............................................................ 1
Work Performed ......................................................... 3
3rd Quarter 1999 ...................................................... 3
4th Quarter 1999 ................ · ...................................... 4
System Performance ................................................. , .... 5
Inner and Outer Tier Extraction Rates ...................................... 5
Ground-Water Movement ............................................... 6
Treatment Efficiencies .................................................. 7
Maintenance Activities ................................................. 8
Analytical Test Results ................................................ , .... 9
Data-Quality Assessment ............................................... 9
Discussion of Analytical Test Results .............. , ....................... 9
Review of Selected Historical Water-Quality Data ........................... 11
Closing Comments ................................................. , .... 14
Tables
Table 1. 1999 Sampling Matrix-CNA Holdings, Inc.-Shelby, NC
Table 2. Inner Tier Production Data (July 1999 -December 1999)
Table 3. Inner Tier TOC Data (July 1999 -December 1999)
Table 4. Summary of Selected CERCLA-related Water-Quality Data (3rd Quarter 1999)
Table 5. Summary of Selected CERCLA-related Water-Quality Data (4th Quarter 1999)
Table 6. Summary of Selected PEW-related Water-Quality Data (3rd Quarter 1999)
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Figures
Figure 1. Site Plan Showing Monitoring Locations and Geologic Cross Sections
Figure 2. Potentiometric Surface Map-Shallow Saprolite-July 20, 1999
Figure 3. Potentiometric Surface Map---Deep Saprolite/Upper Bedrock-July 20, 1999
Figure 4. Hydrogeologic Cross Section A-A', July 20, 1999
Figure 5. Potentiometric Surface Map-Shallow Saprolite--Dctober 21, 1999
Figure 6. Potentiometric Surface Map---Deep Saprolite/Upper Bedrock--Dctober 21, 1999
Figure 7. Hydrogeologic Cross Section A-A', October 21, 1999
Attachments
Attachment 1. Operation and Maintenance Data (July 1999 -December 1999)
Attachment 2. Analytical Data for the 3rd and 4th Quarter 1999 Sampling Events
Attachment 3. Selected Water-Quality Plots
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CNA Holdings, lnc.~5helby, NC-Semiannual Report/Page I
Introduction
CNA Holdings, Inc. (formerly known as Hoechst Celanese Corporation) is currently operating
a long term remedial action (LTRA) system at its Shelby, North Carolina facility. This system,
designated as Operable Unit 1 (OU-1) in the Record of Decision (ROD), consists of two ground-
water extraction and treatment systems identified as the Inner Tier and Outer Tier systems. OU-1
became operational in August 1989.
On April 21, 1998, the Outer Tier portion of OU-1 was shut down as part of a partial de listing
petition approved by the EPA effective April 17, 1998. Active ground-water recovery and treatment
is currently only taking place at the Inner Tier which was designed to extract contaminated ground
water from around a former source area remediated as a separate operable unit (OU-2) with its own
ROD. Although the Outer Tier is not actively recovering ground water, Outer Tier well OT-IR is
still pumped to provide make-up water for the SBR (sequencing batch reactor) and for process
water used for backflushing filters. The entire Outer Tier is being maintained in "stand-by status"
as part of the delisting process and can be brought on line within a relatively short period of time
(24-48 hours) if it is found necessary to provide hydraulic control along the property boundary.
Kubal-Furr & Associates (KF&A) has prepared this semiannual OU-1 operating summary
report for submittal to the EPA on behalf of CNA. It covers the period from July 1, 1999 through
December 31, 1999 and includes information on system performance and the results of analytical
testing of samples collected on July 21-22, 1999, August 18, 1999, October 20, 1999, and
November 9, 1999. (During both the 3rd and 4th Quarter, the laboratory failed to analyze the Inner
Tier influent and effluent samples for ethylene glycol within the prescribed holding times. As a
result, the lab collected additional Inner Tier samples on August 18, 1999 and again on November 9,
1999 for analysis of ethylene glycol.)
Routine ground-water extraction and treatment continued during the semiannual reporting
period. The most significant, non-routine event was the preparation of the draft Five Year Review
Report which was submitted to the EPA and the State of North Carolina during December of 1999.
This report is currently under review.
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CNA Holdings, Jnc.---Shelby, NC-Semiannual Report/Page 2
Work Performed
As part of the OU-1 remedy, samples are collected at selected monitor wells and at points in the
ground-water treatment system. In addition, samples were collected from the PEW extraction well
system and PEW-related monitor wells. A list of sampling locations and the parameters analyzed
during the 3rd and 4th Quarters are summarized in Table 1. A description of the work performed
during this reporting period is provided below.
3rd Quarter 1999
On July 20, 1999, water levels were measured by Kubal-Furr in a total of 91 monitor wells,
extraction wells, and piezometers. A total of 17 water-quality samples and 1 duplicate sample were
collected on July 21-22, 1999 from selected monitor wells and extraction wells. Additionally, 2
process point samples and 1 duplicate were collected. All samples were collected and analyzed by
Davis & Floyd of Greenwood, South Carolina. As previously noted, the laboratory failed to analyze
the ethylene glycols within the accepted holding time and additional samples were collected for
these analyses by the lab on August 18, 1999.
OU-1 Monitor Well Sampling
Thirteen monitor well samples (plus 1 duplicate) were analyzed in the field for pH, temperature
and conductance; and, by the laboratory for volatile organics (VOCs) using EPA Method 82608.
Samples from monitor wells K-28 and V-23 were also analyzed by the laboratory for TOC using
EPA Method 9060.
OU-1 Process Point Sampling
Samples of Inner Tier influent and effluent were collected for analysis of volatile organics by
Method 82608. The Inner Tier influent and effluent samples were also analyzed by the laboratory
for total organic carbon (TOC) by Method 9060, and for ethylene glycol by GC/FID.
During the reporting period, influent and effluent samples from the Inner Tier were also
collected by CNA personnel for analysis of TOC by Davis & Floyd. These samples are collected
weekly to evaluate treatment efficiency, and the results are contained in the O&M reports provided
in Attachment 1. These results are also summarized in Table 3.
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CNA Holdings, /11c.-Shelby, NC-Semia1111ual Report/Page 3
PEW Extraction and Monitor Well Sampling
One PEW-related monitor well (F-55) and 3 PEW extraction well samples (plus 1 duplicate)
were collected during the 3rd Quarter. These samples were analyzed for VOCs by EPA Method
8260B, for SVOCs (semivolatile organics) by EPA Method 8270C (including biphenyl and
diphenyl ether).
4th Quarter 1999
On October 21, 1999, water levels were measured by Kubal-Furr in a total of 91 monitor wells,
extraction wells, and piezometers. Water-quality samples were collected from 2 monitor wells, and 2
process points (plus one process point duplicate) and analyzed for the parameters summarized in
Table 1. The samples were collected on October 20, 1999 by Davis & Floyd, who also performed
the analyses. As previously noted, the laboratory failed to analyze the ethylene glycols within the
accepted holding time and additional samples were collected for these analyses by the lab on
November 9, 1999.
Monitor Well Sampling
Monitor wells K-28 and V-23 were sampled during the 4th Quarter sampling event. These wells
were analyzed in the field for pH, temperature and conductivity; and, by the laboratory for TOC by
Method 9060.
Process Point Sampling
Samples of Inner Tier influent and effluent were collected for analysis of TOC by Method
9060 and volatile organics by EPA Method 8260B. The Inner Tier influent and effluent samples
were also analyzed for ethylene glycol by GC/FID.
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CNA Holdi11gs, lnc.-She/by, NC-Semiannual Report/Page 4
System Performance
Detailed records of system maintenance are kept by CNA and are summarized monthly. The
monthly records for the current reporting period are contained in Attachment 1. Summaries of
physical operating data for the Inner Tier extraction well system is presented in Table 2.
Inner Tier Extraction Rates
During the reporting period, the Inner Tier wells extracted a total of 257,947 gallons. Inner Tier
flows ranged from a low of 39,913 gallons in September, to a high of 47,859 gallons in November.
Pumping from the Inner Tier wells is limited by the capacity of the SBR treatment system, which is
designed to process about 2500 gallons of water per day. With 184 days in the reporting period, at
design capacity, pumping from the Inner Tier would have been some 460,000 gallons. Based on the
pumpage during the reporting period, the Inner Tier extraction system was producing at a rate of
about 56% of the design capacity, which represents a decrease from the previous semiannual
reporting period during which the Inner Tier produced about 69% of the design capacity rate.
Ground-Water Movement
In order to accurately predict the direction of ground-water movement, water-level
measurements were collected from all accessible monitor wells, extraction wells and piezometers on
July 20, 1999 by KF&A, and again on October 21, 1999. These data were used to construct the
potentiometric surface maps and hydrogeologic cross sections (Figures 2 thru 7).
The shallow saprolite maps (Figures 2 and 5) show the water-level contours and direction of
ground-water movement in the uppermost water-bearing zone beneath the site. The direction of
movement in this zone is to the east from upgradient areas along NC 198, towards discharge areas
along the intermittent, unnamed tributaries of Buffalo Creek. Drawdown and a capture zone are
apparent on these figures situated around the Inner Tier extraction system.
An attempt was made to separate the uppermost water-bearing zone from the deeper saprolite
and upper bedrock zone. While these maps (Figures 3 and 6) present a reasonable picture of
ground-water movement in this zone, it should be pointed out that it is giving a somewhat more
generalized picture of ground-water movement because of the well construction techniques used in
many of the wells and piezometers. The typical construction of these wells was to have relatively
long screens (20-40 ft) and extremely long sand packs in the annular space above the screens (up to
60-ft). As a result, the lower saprolite/upper bedrock maps have a number of composite head values
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CNA Holdings, lnc.-Shelby, NC-Semiannual Report/Page 5
measured along a longer screened area, However, the maps may be useful for determining the
general direction of ground-water movement,
To confirm inferences made about the direction of movement and hydraulic control exerted by
the Inner Tier system, hydrogeologic cross sections were constructed from the July and October
data sets (Figures 4 and 7). The location of the cross section is shown on the site base map, Figure
1. The east-west cross section (A-A') is constructed through the plant from upgradient areas west
of the plant to downgradient, off-site areas east of the plant. The east-west hydrogeologic cross
section shows a general direction of movement in the saprolite and upper bedrock from upgradient
areas west of the plant toward downgradient areas to the east, No appreciable downward hydraulic
gradients are apparent on this map, and the movement in the saprolite and shallow bedrock is
predominantly horizontal across the site.
Treatment Efficiencies
Two aspects of the extraction system performance were reviewed for this semiannual report: the
production rates achieved during the reporting period, and the removal efficiencies for TOC from
the Inner Tier system.
Table 3 summarizes the treatment system effectiveness for the Inner Tier in removing TOC
during the reporting period. These summaries were prepared from the water-quality data collected
weekly by the CNA on-site laboratory as presented in the monthly operating summaries
(Attachment 1 ). During the reporting period, the Inner Tier average removal efficiency for TOC was
greater than 99%, with an average influent concentration of 1604 ppm (parts per million), and an
average effluent concentration of 9.5 ppm.
Maintenance Activities
Low flow from the Inner Tier wells is a chronic problem requiring frequent maintenance. The
actions taken to rectify the low flow problems consisted of replacing bladders, timers, air lines and
such, adjusting the controls and flow rates, and cleaning the strainers. Specific actions taken at
individual wells during the reporting period are contained in the monthly operating summaries
(Attachment 1 ).
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CNA Holdings, /nc.--She/hy, NC-Se111ia1111ual Report/Page 6
Analytical Test Results
The analytical test results for the 3rd and 4th Quarter sampling events were evaluated using
method specific quality control criteria and, for additional guidance when necessary, the EPA's
National Functional Guidelines for organic and inorganic data review. Analytical test results, field
sampling logs, and chain-of-custody forms for'the 3rd and 4th Quarter data sets are contained in
Attachment 2. A summary of selected analytical data for the 3rd and 4th Quarters is presented in
Tables 4, 5 and 6.
Data-Quality Assessment
Regarding sample collection, the sampling logs and field information provided were incomplete
but were determined to have no effect on the data. All 3rd and 4th Quarter data were considered
Class A (quantitative) with the following 3rd Quarter exceptions:
• Due to matrix interference, the lab was unable to obtain a clear spectra for selected Inner
Tier and monitor well V-23 analyses. Therefore, the 2-butanone and acetone results for
ITC! and V-23 are flagged with a "J" as estimated. The vinyl actetate results for V-23 also
require a J flag.
• The MS/MSD for sample AA-54 were below established limits and a J flag for associated
constituenys benzene, chlorobenzene, toluene and trichloroethene.
• Although not qualified, it should be pointed out that low levels of methylene chloride were
reported as present in several samples (AA-54, ITEF, ITEF Dupe, K-28, CC-33, PEW-1,
PEW-3, and F-55. The presence of methylene chloride is an uncommon occurrence at CNA
Shelby, and although no contamination was present in either the method blank or trip blank,
methylene chloride is a common laboratory contaminant and its presence in these samples is
considered suspect.
Discussion of Analytical Test Results
CERCLA-Monitor Wells
Of the 13 CERCLA-monitor well samples analyzed during the reporting period, only six had
any volatile organics reported above the detection level (Tables 4 and 5). Of these six, only two (V-
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CNA Holdings, lnc.---Shelby, NC-Semiannual Report/Page 7
23 and K-28) had more than one individual volatile constituent reported as present above the
detection level.
Monitor well V-23, located downgradient of the former OU-2 source area and just upgradient
of the Inner Tier extraction system, reportedly contained acetone (0.271 mg/L), benzene (0.018
mg/L), 2-butanone (0.271 mg/L), and vinyl acetate (0.541 mg/L). Monitor wells HH-48 and HH-
77, off-site and adjacent to the Elliott residence, reportedly contained trichlorothene (TCE) at
concentrations of0.084 mg/Land 0.25 mg/L, respectively. The presence ofTCE at this location is
thought to be the result of a localized source, unrelated to activities at CNA or the former OU-2
source area.
Monitor wells K-28 and V-23 were also analyzed for TOC during the 3rd and 4th Quarters.
The V-23 test results for the 3rd and 4th Quarters were 9620 mg/Land 6930 mg/L, respectively.
The TOC test results for K-28 were noted to increase from 4.4 mg/L to 183 mg/L between the 3rd
and 4th Quarters.
Process Point Samples
Inner Tier influent and effluent samples were analyzed during the 3rd and 4th Quarters for
ethylene glycol, TOC, and volatile organics. All volatile test results for the Inner Tier effluent
sample were below the detection level with the exception of methylene chloride reported at 0.033
mg/L during the 3rd Quarter. Ethylene glycol for the Inner Tier effluent sample during the 3rd
Quarter was reported to be 18 mg/L. Inner Tier effluent TOC was reported as 8.4 mg/L for both the
3rd and 4th Quarters.
The 3rd Quarter Inner Tier influent sample reportedly contained the volatiles acetone (0.0951
mg/L), benzene (0.035 mg/L), chlorobenzene (0.026 mg/L), carbon disulfide (0.011 mg/L) and 2-
butanone (0.052 mg/L). The 4th Quarter Inner Tier influent sample reportedly contained the
volatiles acetone (0.2 mg/L), benzene (0.026 mg/L), carbon disulfide (0.012 mg/L), chlorobenzene
(0.01 mg/L) and 2-butanone (0.037 mg/L). Inner Tier influent ethylene glycol results for the 3rd
and 4th Quarters were reported at 310 mg/Land 1040 mg/L, respectively. Inner Tier influent TOC
results for the 3rd and 4th Quarters were reported at 1530 and 1490 mg/L, respectively.
PEW-Related Samples
Of the four PEW-related samples collected during the 3rd Quarter, only F-55 and PEW-4 had
more than one volatile or semivolatile constituent reported as present. Acetone (0.01 mg/L), benzene
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CNA /folding,; l11c.--She/by, NC-Semiannual Report/Page 8
(0.053 mg/L) and methylene chloride (0.013 mg/L) were reported as present in well F-55. Cis-1,2-
dichloroethene (0.015 mg/L), trichloroethene (0.031 mg/L), and methylene chloride (0.05 mg/L)
were reported as present in PEW-4.
Two of the four wells sampled had reportable quantities of Dowtherm constituents (i.e., 1,1-
biphenyl or biphenyl ether). 1,1-biphenyl was reported as present in wells F-55 (12.4 mg/L), and
PEW-4(0.011 mg/L). Biphenyl ether was reported as present in well F-55 (35.4 mg/L) and PEW-
4 (0.033 mg/L). Well F-55 also reportedly contained the semivolatile constituents dibenzofuran
(0.036 mg/L), naphthalene (0.33 mg/L), phenol (0.033 mg/L), and 4-methylphenol (0.12 mg/L).
Review of Selected Historical Water-Quality Data
Attachment 3 contains plots of selected water-quality constituents for various monitor wells and
process points. The choice of locations and constituents was based on a review of the water-quality
database, in particular those locations having any meaningful data to plot. In general, only those
monitoring locations within a few hundred feet of the former OU-2 source area have any significant
number of water-quality constituents reported above the detection limits. In an attempt to assess
long-term improvement in water-quality conditions resulting from source removal and ground-water
recovery, the following locations and constituents were selected:
• Inner Tier Combined Influent TOC and ethylene glycol test results. The Inner Tier TOC
decreased between the 3rd and 4th Quarter, reversing an increasing trend established in mid-
1997. The Inner Tier ethylene glycol data increased during the 3rd and 4th Quarters
although no long-term trends have been established.
• Monitor Well V-23 TOC, 2-butanone (MEK), acetone and benzene. The V-23 TOC data
began trending downward from a high of 8000 mg/Lin mid-1989 to less than 1000 mg/Lin
early 1992. Since that time, the TOC data have shown several wide swings in concentration.
TOC concentrations at V-23 increased during the 3rd Quarter and declining significantly
during the 4th Quarter.
The V-23 MEK data have generally fluctuated in a narrow range below 1 mg/L, with 11 of
30 data points below the detection level. The values for MEK decreased during the 3rd
Quarter sampling event but no discernable trend is apparent in the data set.
The V-23 acetone test results have generally fluctuated in a narrow range below 0.6 mg/L
since 1989. Acetone concentrations at V-23 have been below the detection level in three of
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CNA Holdings, lnc.-Shelby, NC-Semiannual Report/Page 9
the past five quarters with the other two quarters flagged as estimated due to a matrix
interference.
While more than half the benzene data for V-23 is flagged as estimated or below the
detection limit, the past nine sampling events have been quantitative and show benzene to be
fluctuating in a narrow range of from 10 to 30 µg/L.
Monitor well K-28 TOC and benzene data. TOC and benzene have both shown a stairstep
decrease in concentration beginning about the time the OU-2 source remediation began in
January of 1991. While benzene has shown a general decline during this period, a slight
upward trend noted since the 3rd Quarter of 1997 appears to have stabilized during the past
two quarters.
Monitor well HH-48 and HH-77 TCE data. The HH-48 TCE test results have declined
from a concentration of 0.222 mg/L in August of 1995, to 0.084 mg/L during the most
recent quarter (3rd Quarter 1999). HH-77 had been fluctuating in the range of 0.05 to 0.15
mg/L until the July 1996 sampling event when it peaked at 0.383 mg/L. TCE at HH-77 was
noted to decrease from 0.225 mg/L to 0.13 mg/L between the 3rd Quarter of 1998 and the
1st Quarter of 1999 but has since increased back up to 0.25 mg/L during the 3rd Quarter
1999.
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CNA Holdings, Jnc.-Shelby, NC-Semiannual Report/Page JO
Closing Comments
The extraction well production data and the analytical test results for the monitor wells and
process points were generally found to be consistent with historical information, and no unusual or
unsuspected contamination was identified during the reporting period. Treatment efficiencies at the
Inner Tier for removal of TOC remained consistently greater than 99%, and no volatiles were
detected in either the 3rd or 4th Quarter Inner Tier effluent samples with the exception of a reported
methylene chloride detection which was noted in the 3rd Quarter but not replicated during the 4th
Quarter sampling event.
The next CERCLA-sampling events are scheduled for the 1st and 2nd Quarters of 2000, with
another PEW-related sampling scheduled for the 1st Quarter. The next scheduled semiannual
report is to be submitted to the agency by September 1, 2000.
Kubal-Furr & Associates
-- ----- - - --- --- - --Table 1. 1999 Sampling Matrix-CNA Holdings, lne.-Shelby, NC
1st Quarter 2nd Quarter 3rd Quarter 4th Quarter
Monitoring TOe voe Eth. Glycol TOe voe Eth. Glycol TOe voe Eth. Glycol TOe voe Eth. Glycol
Location (9060) {82608) (GC/FID) (9060) (82608) (GC/FID) (9060) (82608) (GC/FID) (9060) (8260B) (GC/FID)
Process Points
ITCI ,/ ,/ ,/ ,/ ,/ ,/ ,/ ,/ ,/ ,/ ,/ ,/
rTEF ,/ ,/ ,/ ,/ ,/ ,/ ,/ ,/ ,/ ,/ ,/ ,/
om ,/ OT Pumg:ing Discontinued on 4/21/98}
01EF ,/
SBR Sludge (Full TCLP)'1
FP Sludge (Fu!I TCLP)11
Monitor Wells
C-49 ,/ ,/
K-28 ,/ ,/ ,/ ,/ ,/ ,/
P-58 ,/ ,/
T-35 ,/ ,/
V-23 ,/ ,/ ,/ ,/ ,/ ,/
AA-54 ,/ ,/
CC-33 ,/ ,/
EE-58 ,/ ,/
FF-34 ,/ ,/
FF-62 ,/ ,/
GG-61 ,/ ,/
HH-48 ,/ ,/
HH-77 ,/ ,/
voe svoc voe svoc
(82608) (8270C) (8260B} (8270G}
PEW-Related Same_les
PEW-1 ,/ ,/ ,/ ,/
PEW-3 ,/ ,/ ,/ ,/
PEW-4 ,/ ,/ ,/ ,/
B-34
F-55 ,/ ,/ ,/ ,/
G-50
G-88
H-59
H-79
Notes: 1/ TCLP Analyses as speafied in Attachment 2 of most current, approved Sampling & Analysis Plan (KF&A, April 1998)
CNA Holdings, lnc.--Shelby, NC
OU-I Semiannual Report (July '99 -Dec. '99)
-
--
~
IT-1
IT-2
IT-3
IT-4
IT-5
IT-6
IT-7
IT-SR
IT-9
*ADF:
-----
July 1999 August 1999
Total Total
Gallons ADP Gallons ADP
1,576 51 1,635 53
704 23 637 21
1 042 34 1 574 51
2,087 67 2,049 66
7,698 248 6,761 218
1 286 41 1 002 32
3,294 106 2,869 93
13,184 425 15,771 509
16 554 534 8 679 280
47,425 40,977
--- -
Table 2. Inner Tier Production Data
July '99 •· Dec. '99
CNA Holdings, lnc.-Shelby, NC
September 1999 October 1999
Total Total
Gallons ADF* Gallons ADP
2,031 68 1,650 53
716 24 671 22
2 039 68 2 125 69
2,420 81 2,170 70
6,169 206 8,533 275
2 523 84 2 405 78
3,262 109 2,994 97
12,044 401 12,487 403
8 709 290 8 259 266
39,913 41,294
Average Daily Flow based on CNA production records (Attachment 1),
Calculated as total flow divided by the number of days in the month.
--...
November 1999
Total
Gallons ADP
1,547 52
635 21
2,382 79
2,487 83
7,735 258
2 225 74
3,322 111
10,875 363
16 651 555
47,859
- - --
December 1999 Jan,-June '99
Total
Gallons ADF* Total Gallons
1,473 48 9,912
547 18 3,910
2,910 94 12 072
2,155 70 13,368
6,066 196 42,962
1 -~70 60 11 311
3,808 123 19,549
11,520 372 75,881
10,130 327 68 982
40,479 257,947
CNA Holdings, lnc.-Shelby, NC
OU-1 Semiannual Report (July '99 -Dec. '99)
-
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Table 3. Inner Tier TOC Data
July '99 --Dec. '99
CNA Holdings, lnc.-Shelby, North Carolina
(all results reported in ppm)
Influent
Date
7/7/99 1380
7/14/99 1450
7/22/99 1370
7 /28/99 1210
........... 8/4/9.9. 1380
8/11 /99 2920
8/18/99 1360
8/25/99 1220
···········9/.1./9.9 ..................... 1.240 .............. .
9/8/99 2130
9/14/99
9/23/99
9/29/99
1530
1410
2210
Effluent % Reduction
8 99.4
8 99.4
9 99.3
1 1 99.1
7 99.5
8 99.7
8 99.4
8 99.3
7 99.4 ····································•································ 6 99.7
8
4
8
99.5
99.7
99.6
......... 1. o I 6/ 9.9 ..................... 2 05 0 ................................ 9. ..................................... 9..9..:.~ ........... .
1 0/14/99 1980 9 99.5
1 0/20/99
10/27/99
1160
1180
9
10
99.2
99.2
......... 1. 1 /3 /9.9 ..................... 1.1. 60 ............................... 1 .. 1 ................................... 99 .. 1 ........... .
11/9/99
11/17/99
11 /24/99
1180
1290
1350
1 0
7
7
99.2
99.5
99.5
......... 1. 2/ 1./ 9.9 ..................... \~.?..Q ............................... ! . .Q .................................. 9..9..:.? ........... .
12/7/99 2050 11 99.5
12/15/99
12/22/99
12/28/99
Average:
1490
1860
3210
1604
16
18
19
9.5
98.9
99.0
99.4
99.4
CNA Holding,; Inc.--Shelby, NC
OU-I Semiannual Report (July '99 -Dec. '99)
----------- - --- - - - -
Table 4. Summary of Selected Water-Quality Constituents (3rd Quarter 1999)
(All results reported in milligrams per liter)
AA-54 CC-33 K-28 V-23 HH-48
Total Organic Carbon NA11 NA 4.4 9620 NA
Ethylene glycol NA NA NA NA NA
Volatile Organics
Acetone <0.010 <0.010 <0.010 0.27J <0.010
Benzene <0.005J21 <0.005 0.010 0.018 <0.005
2-butanone (MEK) <0.010 <0.010 <0.010 0.27J <0.010
Carbon disulfide <0.005 <0.005 <0.005 <0.005 <0.005
Chlorobenzene <0.005J <0.005 <0.005 <0.005 <0.005
Methylene chloride 0.032 0.011 0.03 <0.005 <0.005
Trichloroethane <0.005J <0.005 <0.005 <0.005 0.084
Vinyl acetate <0.010 <0.010 <0.010 0.54J <0.010
Notes: 1 / NA = Sample not analyzed for indicated constituents
2/ J = Estimated value
HH-77
NA
NA
<0.010
<0.005
<0.010
<0.005
<0.005
<0.005
0.25
<0.010
Inner Tier Inner Tier
Influent Effluent
1530 8.4
310 1 8
0.095J <0.010
0.035 <0.005
0.052J <0.010
0.011 <0.005
0.026 <0.005
<0.005 0.033
<0.005 <0.005
<0.010 <0.010
CNA Holdings, lnc.~helby, NC
OU-/ Semiannual Report (July '99-Dec. '99)
------~------------
Table 5. Summary of Selected Water-Quality Constituents (4th Quarter 1999)
(All results reported in milligrams per liter)
K-28 V-23
Total Organic Carbon 183 6930
Ethylene glycol NA 11 NA
Volatile Organics
Acetone NA NA
Benzene NA NA
2-butanone (MEK) NA NA
Carbon disulfide NA NA
Chlorobenzene NA NA
Notes: 1 / NA = Sample not analyzed for indicated constituent(s)
Inner Tier
Influent
1490
1040
0.2
0.026
0.037
0.012
0.01
Inner Tier
Effluent
8.4
<7.0
<0.010
<0.005
<0.005
<0.005
<0.005
CNA Holdings, Jnc.-Shelby, NC
OU-1 Semiannual Report (July '99 • Dec. '99)
Table 6. Summary of Selected PEW-Related Water Quality Constituents (3rd Quarter 1999)
(All results reported in milligrams per liter)
F-55
Semivolatile Organics
1, 1 bi phenyl 12.4
Biphenyl ether 35.4
dibenzofuran 0.036
naphthalene 0.33
phenol 0.033
4-methylphenol (p-cresol) 0.12
2-methylnaphthalene <0.010
Volatile Organics
Acetone 0.01
Benzene 0.053
cis-1 ,2-dichloroethene <0.005
Methylene chloride 0.013
Trichloroethene <0.005
PEW-1 PEW-3
<0.010 <0.010
<0.010 <0.010
<0.010 <0.010
<0.010 <0.010
<0.010 <0.010
<0.010 <0.010
<0.010 <0.010
<0.010 <0.010
<0.005 <0.005
<0.005 <0.005
0.0071 0.02
0.0066 <0.005
PEW-4
PEW-4 (Dupe)
0.011 <0.010
0.033 0.026
<0.010 <0.010
<0.010 <0.010
<0.010 <0.010
<0.010 <0.010
<0.010 <0.010
<0.010 <0.010
<0.005 <0.005
0.015 0.015
0.031 0.036
0.05 0.049
CNA Holdings, lnc.-Shelby, NC
OU-1 Semiannual Report (July '99 -Dec. '99)
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IT-SR = 787 .66
IT-9 = Not Measured
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Fjqure 2-Potcntiometric Surface Map
SM/low 5.tpn;,liu-July 20, 1999
Celani:5e North "mcnca, Inc.
Shelby, Ncr-th C,11,-ofjna
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(dHl>ecl"""'"'O'llsr..:!)
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Inferred direction of ground-water
movement
- --
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IT-1 = <781.24
IT-2 = <776.40
IT-3 = 774.61
IT -4 = <778.43
IT-5 = 779.11
IT-6 = 777.40
IT-7 = 788.02
IT-8R = 794.99 > >,. >. IT-9 = Nol Measured ~ 't? ~o ',----~-------------< ',:x ',-_;<\
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Shelt,y, NortJi Carolina
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De,,p ~aproljt-e/1Jp~r Bedroc<-Octci=' 21, 1999 c.,;,,,,,..,Nor<J,~.l""-$1,eil,y.N~C,,,.,,...,.
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730.00
710 00
690 00
670.00
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{das-wr,...., inferred) ~ Bedrock
Saprolite ! Potentiometric Surface
Inferred direction of ground•water
movement
Screened Interval of Well Kubal-Furr & Associates
-Environmental Consultants -
Figure 7-Hydroq..,oloiJic Cro,;s-5..ction
kN--Dctot>u 21, 1999
CeJa~ NO,U, ,',m..,nca, Inc.
Shdl,y. Ncrt-h Carolina
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I Attachment 1
I Operation and Maintenance Data
I January-June, 1999
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I Kubal-Furr & Associates ·
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GROUNDWATER MONTHLY MONITORING:
RAINFALL DATA
l JULY
DATE INCHES/DAY
07/01/99 0.00
07/02/99 0.00
07/03/99 0.00
07/04/99 0.00
07/05/99 0.00
07/06/99 0.00
07/07/99 1.00
07/08/99 0.00
07/09/99 0.00
07/10/99 0.60
07 /11/99 0.20
07/12/99 0.70
07/13/99 0.00
07/14/99 0.00
07/15/99 0.00
07/16/99 0.00
07/17/99 0.00
07/18/99 0.00
07/19/99 0.00
07/20/99 0.00
07/21/99 o.oo
07/22/99 0.00
07/23/99 0.00
07/24/99 1.10
07/25/99 o.oo
07/26/99 o.oo
07/27/99 0.00
07/28/99 0.00
07/29/99 0.00
07/30/99 0.00
07/31/99 0.00
TOTAL 3.60
000001
I
INNER TIER I DAILY FLOW
JULY I
1999 IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9
07/01/99 1 21 4 56 248 37 82 402 550 I 07/02/99 66 31 19 65 279 44 84 441 3
07/03/99 65 25 17 77 288 49 92 473 0 I 07/04/99 64 14 42 74 293 47 96 451 631
07/05/99 66 32 41 70 190 46 90 401 595
07/06/99 46 16 21 36 148 27 51 234 378
07/07/99 58 33 34 54 265 40 85 425 615 I 07/08/99 65 26 32 58 283 44 121 459 682
07/09/99 66 28 22 57 272 47 115 459 693
07/10/99 51 22 12 46 234 35 98 356 521
07/11/99 69 31 23 54 200 43 110 135 650 ~ 07/12/99 64 26 12 58 246 46 118 750 694
07/13/99 51 15 0 56 194 38 98 1078 574
07/14/99 62 31 0 63 218 39 105 0 615
07/15/99 61 13 0 66 246 46 121 354 691 I 07/16/99 59 34 33 68 243 45 121 572 689
07/17/99 47 21 42 54 189 33 89 422 498
07/18/99 61 28 53 63 225 35 105 499 101 I 07/19/99 60 27 52 68 257 41 120 579 639
07/20/99 58 26 48 67 276 42 116 565 0
07/21/99 48 25 54 69 272 40 110 542 590
07/22/99 45 27 42 74 255 38 106 360 617
,_J 07/23/99 48 27 50 81 268 42 18 109 656
07/24/99 54 17 53 87 295 48 228 255 747
07/25/99 3 12 45 76 245 47 109 193 627
07/26/99 0 34 49 83 284 49 114 215 694 I 07/27/99 0 30 48 86 286 44 124 209 682
07/28/99 56 26 50 83 278 39 119 524 643
07/29/99 62 6 47 81 253 38 117 545 624
07/30/99 60 0 49 79 238 39 116 594 614 J 07/31/99 60 0 48 78 230 38 116 583 241
AVG: 51 23 34 67 248 41 106 425 534 I TOTAL: 1576 704 1042 2087 7698 1286 3294 13184 16554
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MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
ACTION
DATE WELL# PROBLEM DATE ACTION
7/16/99 #3 LOW FLOW 7/16/99 CLEANED SUPPLY LINE
7/19/99 #9 LOW FLOW 7/19/99 ADJUSTED CONTROL
7/21/99 #9 LOW FLOW 7/21/99 RESET CONTROLS
7/27/99 #1 NO FLOW 7/28/99 NEW PUMP &CLEANED LINE
7/27/99 #8 LOW FLOW 7/28/99 NEW PUMP & CHANGED EXHUASTER
7/30/99 #2 NO FLOW 7/30/99 CLEANED PROBE
000003
MECHANIC
L.B.
L.B.
L.B.
L.B.
L.B.
L.B.
Quarterly O&M Plan Checklist-HNA Holdings, lnc./Shelby, NC Form Completed by: TONY BRYANT
Date: 7/1 /99
Open Sample Energize Verify De-energize Close Sample Verify Heater Secure Well
Port Pump Discharge Pump Port Operation Vault Comments
Outer Tier Well
OT-2R X X X X X X X
OT-3 X X X X X X X
OT-4 X X X X X X X
OT-5 X 0 X X X X X X
0
0 OT-6 X X 0 X X X X X
0 ,.:. OT-6A X X X X X X X
OT-7 X X X X X X X
OT-8 X X X X X X X
..
,.__;_A~,,;..
Energize Energize Energize Energize Energize
Ground-Water AS Blower Transfer Pump Transfer Pump Transfer Pump Transfer Pump
Treatment Sys. Y-V-1008 Y-P-1007A Y-P-10078 Y-P-1008A Y-P-10088 Comments
-------- -
la.I -------- - --
I
I DAILY REFERENCE SHEET:
I DATE: IT. EQ. PLT. DEC. DEC. WAS MIX MIX MIX NIT PHOS MIX F/M
JULY. INF. TNK. SEP. LIQ LIQ LIQ ADD ADD LIQ WAS 5/DAY
1999 COD. COD. COD. COD. TSS. TSS MLSS Jill PHOS GALS LBS SET. GALS F/M AVG.
I 1 3630 2990 8120 1392 148 16.0 0 2 130 67 0.00
2 3250 3230 4100 127 68 8350 1440 77 33.6 1 0 150 67 0.25
3 4270 3590 3160 140 48 2390 1328 141 20.0 0 0 125 50 0.21
4 6500 4560 1380 108 13.3 1 130 0 0.00
I 5 3780 2930 4200 150 32 1412 115 26.0 0 130 0 0.26 0.15
6 4470 4640 1428 94 34.8 0 110 0 0.00 0.15
7 4460 4600 5020 134 32 9010 1284 112 23.6 0 120 54 0.35 0.16
8 3840 2640 3620 118 44 1508 108 13.2 0 1 110 0 0.21 0.17
9 3180 3030 3620 98 36 9380 1560 91 31.2 1 0 120 54 0.21 0.21
I 10 4510 4150 1632 103 22.0 1 0 120 0 0.00 0.15
11 3550 3490 3250 143 40 1436 162 12.0 0 1 120 0 0.20 0.19
12 3640 3340 3870 118 48 3400 1564 117 24.0 1 1 140 54 0.22 0.17
13 3360 2660 8830 1688 122 25.6 0 0 140 54 0.00 0.13.
I 14 4090 3680 3890 101 4 4300 1836 114 28.0 0 150 54 0.19 0.12
15 3370 4090 3470 164 28 4880 1400 175 16.0 0 2 150 54 0.22 0.17
16 3940 3740 3780 118 20 9520 1512 109 22.8 0 0 150 54 0.22 0.17
17 4830 4490 1664 100 20.4 0 150 0 0.00 0.13
18 4570 4410 3190 125 67 8670 1572 108 20.0 0 0 150 81 0.18 0.16
I 19 4310 3550 4180 134 10 10080 1612 91 12.8 2 150 54 0.23 0.17
20 5230 4550 4400 120 36 9210 1440 106 18.0 1 150 81 0.27 0.18
21 6680 4780 4600 1608 106 17.4 1 150 81 0.00 0.14
22 3710 4080 3380 120 50 7970 1208 143 18.0 0 1 150 81 0.25 0.19
I 23 5300 4680 3360 114 28 8250 1592 116 20.0 1 2 150 81 0.19 0.19
24 4220 4010 1480 180 20.0 0 0 150 0 0.00 0.14
25 3280 3570 3520 107 20 11880 1372 197 24.0 0 0 140 120 0.23 0.13
26 4730 4040 3480 104 28 9700 1600 167 12.0 0 2 140 120 0.19 0.17
27 4520 4320 9200 1740 103 21.2 0 0 120 135 0.00 0.12
I 28 4490 4610 3110 94 12 8380 1424 94 22.4 120 135 0.19 0.12
29 3750 3640 4090 120 20 8370 1988 119 20.0 1 120 135 0.18 0.16
30 3920 3000 2910 88 4 1100 1540 108 20.1 0 0 120 135 0.17 0.15
31 3980 3380 11790 1260 102 16.0 120 135 0.00 0.11
I AVG: 4237 3828 3527 115 31 7712 1514 120.5 20.8 1 1 135 62 0.15 0.10
MAX: 6680 4780 5020 164 68 11880 1988 197.0 34.8 1 2 150 135 0.35 0.13
MIN: 3180 2660 0 0 0 1100 1208 77.0 12.0 0 0 110 0 0.00 0.10
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I 000005
GROUNDWATER MONTHLY MONITORING:
INNER TIER COMBINED INFLUENT #2 ITCI SBR MIXED LIQUOR: SBRML
PAGEN0.1 PAGEN0.4
JULY.1999 JULY.1999 SETT. SLUDGE SIOAY DATE· FLOW PH: COO: TSS: TOC· DATE PH NH3N: P04: DQ MLSS: MLVSS· SOLIDS WASTED FIM: F/M: GPO pH ppm ppm ppm pH ppm ppm ppm ppm ppm mla '" ratio ratio
07/01199 1401 S4 '630 9 07A'.l1197 8.1 148 16.0 1.4 1392 130 67 0.00
07102199 2089 S3 3250 8 07/02197 8.1 77 33.6 2.2 1440 1SO 87 0.25
07103199 1086 S.3 4270 8 07/03/97 8.1 "' 20.0 1.9 1328 125 so 0.21
07/04199 1712 S.3 8S00 8 0710-4/97 8.1 2.1 1380 130 0 0.00
07/05/99 1531 S.3 3780 8 07/05197 8.1 115 2'0 2.S 1412 130 0 0.26 0.15 07/06/99 957 5.3 «70 9 "''°""' 8.1 " 34.8 2.1 1428 1124 110 0 0.00 0.15
07/07199 1009 S.2 -8 1380 07/07/97 8.1 112 23.6 2.1 1284 120 " 0.35 0.16 07/08/99 mo S.3 3840 07/06197 8.2 108 13.2 2.8 1508 110 0 0.21 0.17
07/09/99 1759 5.3 3180 10 07/09/97 8.0 91 31.2 24 1560 120 " 0.21 0.21 07/10199 1375 5.3 4510 12 07110197 8.1 103 22.0 2.0 1632 120 0 0.00 0.15 07111199 # 1315 5.2 35SO 6 07/11197 8.2 182 12.0 2.1 1438 120 0 0.20 0.19 07/12199 2014 S.3 3840 1S 07/12197 8.1 117 24.0 2.1 1564 140 " 0.22 0.17
07/13/99 2104 5.3 3380 7 07/13197 8.1 122 25.6 2.3 1888 140 " 000 0.13 07114/99 1133 S.2 ,o,o 1S 1450 07114/97 8.1 , " 28.0 2.8 1838 1488 1SO " 0.19 0.12 07115/99 1598 5.3 3370 6 07/15/97 8.1 175 18.0 2.1 1400 1SO " 0.22 0.17
07116199 '"' ,., 39'0 11 07/16197 8.1 109 22.6 2.8 1512 1SO " 0.22 0.17 07/17199 1395 S.3 4630 s 07/17197 6.0 100 20.4 2.5 1884 1SO 0 0.00 0.13
07116/99 1170 S.2 4570 13 07/16197 8.1 108 20.0 2 1 1572 1SO 81 0.18 0.16 07119/99 1843 S.2 4310 17 07119/97 6.1 91 12.8 2.2 1612 1S0 " 0.23 0.17 07/20/99 1198 S.2 5230 18 07'20197 8.1 108 18.0 2.0 1«0 1184 ,so 81 0.27 0,18 0 07/211,19 17SO S.2 6680 2 07'21197 8.1 108 17.4 2.S 1608 ,so 81 000 0.14
0 07122199 1584 5.2 3710 s 1370 01a2191 8.2 '" 18.0 2A 1208 ,so 81 0.25 0.19 07/23/99 1299 S.1 5300 ' 01a,3197 6.1 118. 20.0 2A 1592 ,so 81 0.19 0.19
0 07124199 1784 S.2 4220 11 07'24197 6.1 180 20.0 2.3 1480 1SO 0 000 0.14 07/25/99 1357 S.1 3280 7 O?a.5197 6.1 197 24.0 24 1372 140 120 0.23 0.13 0 07'2&,9 1522 S.3 4730 1S 07/26/97 6.1 187 12.0 2.7 1600 140 120 0.19 0.17
0 07/27199 1510 S.2 4520 20 07/27/97 8.1 103 21.2 24 1720 1352 120 135 0.00 0.12 07128/99 1818 53 «90 10 1210 O?a.6197 8.1 " 22.4 2.9 1424 120 135 0.19 0.12 ,::1) 07/29199 ,m 5.2 3750 6 07129197 8.2 119 20.0 2.7 1988 120 13S 0.18 0.16 07130199 1789 5, 3920 10 07/30197 8.2 108 20.1 2.1 15'0 120 13S 0.17 0.15 07131199 1394 5.3 3980 15 07/31197 82 102 16.0 1.8 1260 120 135
AVG 1563 5.3 4237 10 1353 AVG: 8.1 121 21 2 1514 1289 135 62 0.15 0.18 MAX 21Cl< " 6680 20 1450 MAX: 8.2 197 35 3 1988 1496 ,so 135 0.35 0.21 MIN. 957 5, 3180 2 1210 MIN 8.0 77 12 1 1208 1124 110 0 0.00 0.12
-- --- - -- - - -- - ----
---- --- - ------- ----
GROUNDWATER MONTHLY MONITORING: GROUNDWATER MONTHLY MONITORING: AFTER PLATE SEPARATOR BEFORE SBA: SBRI SBA EFFLUENT:(DECANT) #4 SBRE PAGE NO. 3 PAGE NO. 5 JULY.1999 JULY.1999 WAS. NHJN PHOS. DATE: PH: COD: TSS· DATE: FLOW: COD: TSS:TSS ADDEO: ADDED: pH ppm ppm GPO ppm ppm ppm ,. "' 07/01199 07I01/99 0 8120 0 2 07/0'l/99 6.2 4100 26 07/02199 2009 127 66 8350 , 0 07103/99 71 3160 16 07/03199 24'2 140 46 2390 0 0 07/04/99 0711)4/99 0 ,
07/05199 6.7 <200 6 07/05199 , .. , ,so 32 0 07"""99 07/06/99 0 0 07107/99 6.• 5020 24 07/07/99 2469 134 32 9010 , 0 07/08199 72 3620 40 07/08/99 2473 ,,. ... 0 ,
07/09/99 5.9 3620 26 07/09/99 2403 98 "' 9360 0 07/10/99 07/10/99 , 0 07111/99 6.7 3250 24 07/11/99 2096 1'3 40 0 07/12199 S4 3870 ,. 07/12/99 2'63 ,,. 46 3400 ,
07/13/99 07/13199 0 8830 0 0 07/1-4/99 5.3 3890 4 07/14199 2213 101 4 4300 0 07/15199 5.6 3470 20 07/15199 2413 164 26 4660 0 2 07116199 5.8 3780 8 07/16199 2213 ,,. 20 9520 0 0 07117199 07/17/99 0 , 0 07118199 S.8 3190 26 07118199 2168 125 67 6870 0 0 07119/99 S.9 4160 12 07/19199 2371 134 10 10080 2 07120/99 S.6 4'00 16 07l20/99 201' 120 "' 9210 0 07'21199 07121.W 0 4600 0712.2/99 S.4 3380 6 07122/99 1979 120 50 7970 0 , 0 07123199 S.7 3360 20 07123199 2370 114 26 8250 , 2 0 07124199 07124199 0 0 0 07125199 54 3520 24 07/25199 1968 107 20 11880 0 0 0 07126199 6, 3460 46 07""99 2409 104 26 9700 0 2 0 07/27199 07127/99 0 9200 0 0 07128199 S.4 3110 24 07128199 1875 94 12 6380 -•.J-. 07129199 5.S <090 24 07"""9 232S 120 20 8370 , ,
07130/99 5.4 2910 6 07/3-0/99 2189 " 4.0 1100 0 0 07131199 07'31/99 0 11790 ,
AVG S.9 Je9s 20 AVG: 1551 ,,, 32 m2 ,
MAX: 7.2 5020 46 MAX· 2473 164 88 11880 , 2 MIN: 5.3 2910 4 MIN: 0 " 4 1100 0 0
DID NOT PROCESS SBR.
GROUNDWATER MONTHLY MONITORING: GROUNDWATER MONTHLY MON!TORIN"
INNER TIER EQUALIZATION TANK: ITEQT INNER TIER CARBON Fil TER EFFLUENT #8 ITEF
PAGE NO. 2 PAGE NO. 7
JULY.1999 JULY.1999
DATE· PH: COD; OT WATER ADDED DATE: PH: COD: TDC: TS$:
pH ppm gal pH ppm ppm ppm
07/01199 7.6 2990 07/01/99
07/02/99 7.7 3230 07/02199
07/03199 7.7 3590 07/03199
07/04199 7.6 4560 07/04199
07/051'99 7.5 2930 07/05199
07"6199 7.7 "" 07/0MS
07/07199 7.5 ... oo 07/07199 6.1 146 6 60
07/08199 7.6 21340 07/08199
07/09199 7.6 3030 300 07/09/99
07110,'99 7.7 4'50 07/10/99
07111/99 7.6 3'90 07/11/99
07/12/99 7.6 3340 07/12/99
07/13/99 7.6 2660 07/13199
07114/99 7.6 3660 07/14199 6.2 " 07/15199 7.7 ,090 07/15199
07116/99 7.5 3740 525 07/1!3199
07117/99 7.6 4'90 07/17/99
07116/99 7.6 4'10 07118/99
07/19199 7.5 3550 375 07/19/99
07120'99 7.7 4550 450 07/20199
07/21/99 7.7 '760 07121/99
0 07/22199 7.6 40130 07/22/99 8.2 " • a 07/23/99 7.7 '860 07/23199
07/24/99 80 4010 07/24199 a 07125199 7.7 3570 07/25199
071213199 6.2 ""0 563 07/26199 a 07!27/99 7.6 4320 07!27/99
a 07!28/99 7.8 '810 07128/99 8.1 108 11
07/29/99 7.8 "" 375 07129/99 co 07130/99 80 3000 563 07/30/99
07/31/99 7.6 3360 07/31199
AVG 7.7 3826 450 AVG· 82 110 ' 42
MAX: 6.2 4760 563 MAlt 82 146 11 60
MIN: 7.5 2600 300 MIN: 6.1 " 6 •
-- -- ---- -- - ----- --..
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GROUNDWATER MONTHLY MONITORING:
RAINFALL DATA
DATE INCHES/DAY
08/01/99 0.00
08/02/99 0.00
08/03/99 0.00
08/04/99 0.00
08/05/99 0.00
08/06/99 0.00
08/07/99 0.00
08/08/99 0.10
08/09/99 o.oo
08/10/99 0.00
08/11/99 0.00
08/12/99 0.00
08/13/99 0.00
08/14/99 0.00
08/15/99 0.00
08/16/99 o.oo
08/17/99 0.00
08/18/99 0.00
08/19/99 0.00
08/20/99 0.70
08/21/99 0.00
08/22/99 0.00
08/23/99 1.20
08/24/99 0.20
08/25/99 0.00
08/26/99 1.00
08/27/99 0.00
08/28/99 0.00
08/29/99 0.00
08/30/99 0.00
08/31/99 0.00
TOTAL 3.20
000009
I
INNER TIER
DAILY FLOW I
AUG. I
1999 IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9
08101199 58 0 50 65 218 31 111 505 104 I
08102199 59 36 48 58 224 38 116 597 485
08103199 45 26 38 48 184 30 89 463 295
08/04199 58 30 55 58 227 35 97 530 474 I 08105199 59 27 52 63 276 41 120 608 611
08/06/99 57 24 52 66 264 39 121 605 561
08/07199 57 24 52 72 228 36 125 597 396
08108199 57 24 51 72 225 34 121 577 105 I 08109199 57 25 50 73 236 36 117 552 14
08110199 55 25 51 71 227 37 120 127 15
08111/99 54 25 50 73 218 35 120 469 55
08112199 54 8 50 79 222 38 125 550 260 I 08113199 54 0 52 74 219 35 128 533 451
08/14199 52 0 50 73 214 37 135 542 441
08/15199 51 0 47 63 206 31 51 488 358
08/16199 52 39 51 70 233 36 44 559 322 I 08117199 52 32 49 68 236 35 41 552 272
08/18199 49 27 45 65 184 25 32 422 200
08/19/99 51 23 47 75 228 33 43 544 286 I 08120/99 49 25 48 69 219 31 35 573 236
08/21/99 50 26 49 59 199 28 31 402 241
08/22/99 50 26 49 59 209 32 8 512 257
08/23199 50 27 48 59 200 32 9 509 261 I 08/24199 47 27 49 53 192 27 18 454 223
08/25/99 50 27 50 64 222 32 84 517 244
08126199 46 14 46 64 199 31 140 475 270
08127199 48 0 61 58 216 27 '127 452 244 I 08128/99 50 0 56 65 229 32 146 503 244
08129199 53 0 58 64 214 31 136 463 119
08/30/99 43 40 59 63 206 30 138 534 348
08/31/99 68 30 61 86 187 7 141 557 287 I
AVG: 53 21 51 66 218 32 93 509 280
TOTAL: 1635 637 1574 2049 6761 1002 2869 15771 8679 I
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000010 I I
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MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
ACTION
DATE WELL# PROBLEM DATE ACTION
8/2199 #1 LOW FLOW 8/399 CLEANED SUPPLY LINE
8/2/99 #3 LOW FLOW 813/99 CLEANED SCREEN
8/2/99 #4 LOW FLOW 813/99 CLEANED SCREEN PROBE
8/2/99 #5 LOW FLOW 814/99 ADJUSTED CONTROLS
8/2/99 #6 LOW FLOW 814/99 CHANGED METER
812/99 #7 LOW FLOW 815/99 FIWED AIR LINE & NEW BLADDER
812/99 #8 LOW FLOW 816/99 NEW PUMP
8/9/99 #9 LOW FLOW 8/899 RESET PUMP
8/19/99 EQTANK 8119/99 EQ PUMP REPLACE SEALS
000011
MECHANIC
P.P
P.P.
P.P.
P.P.
P.P
P.P.
P.P.
P.P.
MAX&PURV
I
DAILY REFERENCE SHEET: I
DATE: IT. EQ. PLT. DEC. DEC. WAS MIX MIX MIX NIT PHOS MIX F/M I AUG. INF. TNK. SEP. LIQ LIQ LIQ ADD ADD LIQ WAS 5/DAY
1999 COD. COD. COD. COD. TSS. TSS MLSS NIT PHOS GALS LBS SET. GALS F/M AVG.
1 5700 3200 3180 118 4 8060 1400 119 27.5 0 0 120 135 0.20 I 2 7040 4830 3760 99 32 10160 1268 114 20.0 1 120 135 0.26
3 3780 4160 9150 1568 120 16.0 0 0 120 135 0.00
4 3860 3900 3730 92 36 8750 2160 120 10.0 2 120 135 0.15
5 4040 3450 4030 94 4 8480 1352 118 9.2 1 2 120 135 0.26 0.18 I I
6 3370 3180 4350 93 8 10910 1584 122 11.0 0 2 120 35 0.24 0.19
I 7 3230 2680 2060 100 40 4050 1140 135 16.0 0 0 150 60 0.16 0.16
8 3960 2800 2500 77 24 12290 1940 106 10.4 2 120 60 0.11 0.19
9 4150 3020 3060 124 20 10900 1536 95 16.0 2 140 60 0.18 0.19
10 7630 4980 9120 1596 106 27.2 1 0 140 121 0.00 0.14 I 11 8280 4320 2735 125 20 6550 1564 148 33.3 0 0 140 121 0.16 0.12
12 6150 4220 9920 1404 117 32.0 0 0 120 121 0.00 0.09
13 4330 4780 5040 92 32 8270 1460 124 20.8 0 0 120 121 0.31 0.13
14 4540 5080 9550 1548 104 13.2 1 120 121 0.00 0,09 I 15 4470 4600 4450 84 40 8030 1392 121 19.6 120 121 0.28 0.15
16 4370 3700 5000 110 4 10030 1600 157 16.0 0 0 120 121 0.28 0.17
17 3810 3730 11860 1376 159 14.4 0 2 120 121 0.00 0.17
18 3900 3640 3470 95 16 8170 1156 107 24.0 0 0 120 121 0.27 0.17
19 4020 4180 3740 107 56 9000 1460 130 12.0 0 2 120 121 0.23 0.21 I 20 4330 3540 4900 1552 75 18.5 1 2 120 121 0.00 0.15
21 4080 4490 2810 101 4 8220 1308 115 27.6 120 121 0,19 0.14
22 3650 3300 2930 89 36 8780 1440 105 24.0 120 121 0.18 0.17
23 4720 2940 4360 1640 147 16.4 0 0 120 121 0.00 0.12 I 24 4880 4430 3550 109 60 10190 2108 175 28.6 0 0 120 121 0.15 0.10
25 5030 4260 3960 102 36 13770 1428 109 21.6 1 120 121 0.25 0.15
26 4280 3880 8360 1412 147 11.7 1 1 120 121 0.00 0.12
27 3880 3210 2590 92 20 8870 1376 148 27.2 0 0 120 135 0.17 0.11
28 5480 4580 4100 120 28 9040 1520 122 20.2 0 0 130 135 0.24 0.16 I 29 4990 2500 1568 107 15.0 130 135 0.00 0.13
30 5730 4520 3840 117 88 2310 1408 147 22.0 0 0 140 135 0.24 0.13
31 4480 4030 4790 109 16 11980 1664 103 12.0 0 0 140 135 0.26 0.18
AVG: 4715 3875 3464 98 27 8801 1514 123.3 19.1 0 1 125 117 0.15 I MAX: 8280 5080 5040 125 88 13770 2160 175.0 33.3 1 2 150 135 0.31
MIN: 3230 2500 0 0 0 2310 1140 75.0 9.2 0 0 120 35 0.00
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000012 I
- - -- -- - - ------ ----
GROUNDWATER MONTHLY MONITORING:
INNER TIER COMBINED INFLUENT #2 ITCI SBR MIXED LIQUOR: SBRML PAGE N0.1 PAGE N0.4
AUGUST.1999 AUGUST.1999 SETT. SLUDGE 5/0AY DATE: FLOW. PH: COD: TSS: TOC: DATE: PH: NH3N: POI: oo, MLSS: MLVSS: SOLIDS: WASTED F/M: FrM: GPO pH ppm ppm ppm pH ppm ppm ppm ppm ppm me ,., -"""
08/01/99 1142 5.2 5700 10 08/01199 8.2 119 27.5 2.9 1400 120 135 0.20 08/02/99 1861 5.2 7040 7 06/02199 8.1 114 20.0 2.9 1"'8 120 135 0.2" 08/03199 1218 5.2 3780 8 06/03189 8.2 120 16.0 2.8 1588 1252 120 135 000 08/04199 1564 5.1 3860 12 1380 -8.2 120 10.0 3.5 21eo "° 135 0.15 08/05199 1857 5.3 <040 7 06/05'99 8.2 118 9.2 32 1352 120 135 02" 0.18 0""""9 1789 5.3 3370 • 06I08l99 8.2 122 11.0 3.0 158< 120 35 0.24 0.19 08107199 1587 5.1 3230 5 06/07199 8.1 135 16.0 2.7 1140 150 80 0.16 0.16 08/08/99 1"'8 5.3 3980 11 06/08199 8.2 108 10.4 2., 19<0 120 80 0.11 0.19 08<)1>,99 1160 5.3 4150 5 06/08/99 8.1 95 16.0 2., 1536 1<0 80 0.18 0.19 08/10/99 728 5.2 7830 5 08/10/99 8.2 108 27.2 2.8 1530 1240 1<0 121 0.00 0.14 08/11199 1099 5.0 8280 15 mo 08/11/99 83 , .. 33.3 2.5 1564 140 ,,, 0.16 0.12 08/12199 ,,.. 5.3 6150 8 08/12199 81 117 32.0 3' 1404 120 121 0.00 0,09 08/13199 1548 5.3 '330 17 08/13199 8.2 12' 20.8 31 1480 120 121 0.31 0,13 08/14/99 1544 5.3 <540 10 08114199 8.1 104 13.2 2.8 1548 120 121 0.00 0.09 08/15199 1295 5.3 4470 12 08/10/99 8.2 ,21 19.8 3.2 1392 120 ,,, 0.28 0.15 08/16/99 1408 5.3 4370 12 08/18199 8.2 107 18.0 27 1800 120 "' 0.28 0.17 08/17"39 1337 5.2 3810 • 08/17/99 8.2 159 14.4 3.2 1376 1098 120 "' 0.00 0.17 08118/99 "''' 53 3900 5 1380 08/18199 8.2 107 24.0 2.7 1158 120 121 0.27 0.17 08119"39 1330 5.3 4020 18 08/19'99 8.2 130 12.0 2.9 1480 120 121 0.23 0.21 08'20,'99 1285 5.3 "" 32 08/20/99 8.2 75 18.5 3.1 1552 ,20 ,21 0.00 0.15 08121'99 1085 5.2 ,ooo 5 08/21199 8.3 115 2706.0 3.8 1308 120 121 0.19 0.14
0 Oll/22199 ,202 5.3 3850 8 08/22199 8.3 105 24.0 2.8 1440 120 121 0.18 0.17 08'23199 1195 5.3 mo 5 08/23199 8.3 '" 1!U 3.2 ,a,o 120 ,,, 0.00 0.12 0 08124"39 1090 5., 4880 2 0812<199 8.2 175 288 3.4 2108 1908 120 "' 0.15 0.10
0 08125199 1090 5.< 5030 1220 08/25'99 8.2 109 21.6 2.9 142" 120 ,,, 0.25 0.15 oam,ss 1285 5.1 4280 08/28/99 8.1 "' 11.7 3.4 1412 120 ,,, 0.00 0.12 0 08127"39 1233 5.3 3880 " 08/27199 8.2 148 27.2 2.7 1378 120 135 0.17 0.11 08128/99 1325 5.3 5480 12 08/28199 8.' ,22 20.2 3.0 1520 130 135 0.24 0.16 1-4 08129"39 1138 5.< '990 19 08/29199 8.1 107 15.0 2.7 1588 130 135 000 0.13 w 08/30/99 ,..,, 5.3 5730 10 0813o,gg 8.2 "' 22.0 3.0 1408 1<0 135 0.24 0.13 08131/99 1424 5.< ·-13 08/31/99 8.1 103 12.0 3.8 1864 1276 140 135 028 0.18
AVG: 1315 5.3 4715 10 1720 AVG: 8.2 123 108 3 1512 135' 125 117 0.15 0.15 MAX: 1857 5., 8280 32 2920 MAX 8.3 175 2708 • 2180 1908 ,so 135 0.31 0.21 MIN· 728 5.0 3230 1220 MIN: 8.1 75 9 2 1140 1098 120 35 0.00 0.09
GROUNDWATER MONTHLY MONlTOR\NG GROUNDWATER MONTHLY MONITORING:
AFTER PLATE SEPARATOR BEFORE SBR: SBRI SBR EFFLUENT:(DECAN1) #4 SBRE PAGE NO. 3 PAGE NO. 5
AUGUST.1999 AUGUST.1999 WAS. NH3N PHOS.
DATE: PH: COD: TSS: DATE: FLOW COD: TSS: TSS ADDED ADDED:
pH ppm ppm GPO ppm "'" ppm ,,, '"
08/01199 54 3180 24 08/01/99 1875 118 6060 0 0 08/02199 5.4 3760 52 08/02199 2354 99 32 10160 1 1 08/03199 08/03199 0 9150 0 0 06,104'99 5.6 3730 24 08/04/99 2003 92 36 8750 1 2 08/05199 5.4 4030 16 06/05199 2070 " • 6'60 1 2
08/06/99 54 4350 08/06/99 1875 93 6 10910 0 2 08/07'99 55 2060 24 08/07199 2481 100 " "" 0 0 06/06199 5.5 2500 12 06/06199 2492 77 " ,,,., 2 08/09/99 56 3060 6 08/09199 2438 124 20 10900 2 06'1"'99 06'1"'99 0 9120 1 0 08/11199 5.5 2735 32 08/11/99 2138 125 20 8550 0 0 06/12199 06/12199 0 9920 0 0 06/13/99 5.4 50<0 32 06/13/99 1875 92 32 8270 0 0 08/14199 OB/14/99 0 9550 06/15'99 54 "50 " 06/15199 2177 "" " 6030 1 06/1""9 5.5 5000 12 06/16199 2«1 110 4 10030 0 0 08/17199 08117199 0 11660 0 2
06/16199 5.5 3470 4 06/16'99 2138 95 16 8170 0 0
08119/99 5.9 3740 52 06/19199 2252 106 56 0000 0 2 06/2~99 06'21"99 0 4900 2
0 06Q1/99 5.4 2810 4 06Q1/99 2177 101 • 6220
06/22199 5.7 2930 20 06/22199 2467 69 36 8780 1 0 oam,,. 06Q3/99 0 4360 0 0
0 06Q4'99 5.5 3550 6 06Q4/99 1683 109 60 10190 0 0 08/25199 5.7 3960 24 OSQS/99 2530 102 36 13770
.) """" 06'26199 0 6360 1 1 _. 06Q7'99 5.5 2590 6 ""'"' 1875 92 20 8870 0 0 ' 06/2""9 6.4 4100 12 06Q6199 2366 120 26 9040 0 0 .·..:. OB/29199 06Q9199 0 1 1 ""'~" 5.4 3640 6 """"" 1875 117 66 2310 0 0 08/31199 5.7 4790 12 ""31"9 2390 109 16 11980 0 0
AVG: 5.6 3622 20 AVG: 1557 102 26 6601 0 MAX· 64 5040 52 MAX: 2530 125 68 13770 1
MIN: 5.4 2060 4 MIN" 0 77 4 2310 0 0
DID NOT PROCESS SBR.
- -- ------------ - --
- - -- -- ----- ---- -- --
GROUNDWATER MONTHLY MONITORING: GROUNDWATER MONTHLY MONITORINC: INNER TIER EQUALIZATION TANK: ITEOT INNER TIER CARBON FILTER EFFLUENT #8 ITEF PAGE NO. 2 PAGE NO. 7 AUGUST.1999 AUGUST.1999
DATE: PH: COD: OT WATER ADDED DATE: PH: COO: TOC: TSS· pH ppm "'' pH ppm ppm """'
08101199 7.2 3200 00/01/99 ""1)2199 6.0 4830 0Ml2199 08,03/99 5.1 4160 08,03199 ""4199 5.0 3900 08/04199 8.2 87 7 32 ""1)5/99 7.2 3'50 08,135199
0Wl/99 7.4 3160 525 ™""99 0Ml7199 7.5 2680 08')7199
""""' 7.2 2800 """"' 0M19/99 7.5 3020 563 08')9199
08J10l99 7.8 4980 08/10/99 08J11/99 7.6 4320 443 08/11199 8.3 8 08'12199 7.6 '220 08/12199 08/13/99 7.5 4780 08/13199 08/14199 7.6 5060 08/14199 06/15199 7.4 4800 06/15199 OS,16/99 7.7 3700 243 "'""" 08117199 76 3730 08/17199
OS,16/99 7.3 3640 08/18199 8.2 8
0 OS,19/99 7.5 4180 375 08/18199 0800/99 7.5 3540 OM0/99 0 08121/99 7.3 4490 08/21199
0 osn2199 7.5 3300 168 08/22199 osn3/99 7.5 2940 08/23199
0 08/24199 7.4 4430 0sn4199
osn5'99 7.5 '260 225 Qsn"'9 8.3 6 i-"' Qsn6/99 7.5 3880 Qsn6/99
01 0Sf27199 7.3 3210 Qsn7199
osn8199 56 4580 300 Qsn6199 o,n,m 54 2500 08/2""9
06/30/99 5.4 4520 06/30/99
08'31'99 7.4 4030 285 OM1/99
AVG 7.1 3875 350 AVG: 8.3 87 6 32 MAX 7.7 5060 563 MAX: 8.3 67 8 32 MIN: 5.0 2500 186 MIN· 6.2 67 7 32
GROUNDWATER MONTHLY MONITORING:
RAINFALL DATA
DATE INCHES/DAY
09/01/99 0.00
09/02/99 0.00
09/03/99 o.oo
09/04/99 0.00
09/05/99 2.00
09/06/99 0.00
09/07/99 o.oo
09/08/99 0.00
09/09/99 0.40
09/10/99 0.00
09/11/99 0.00
09/12/99 0.00
09/13/99 0.00
09/14/99 0.00
09/15/99 0.00
09/16/99 0.00
09/17/99 0.00
09/18/99 0.00
09/19/99 0.00
09/20/99 0.00
09/21/99 1.10
09/22/99 0.00
09/23/99 0.00
09/24/99 0.00
09/25/99 0.00
09/26/99 0.20
09/27/99 0.80
09/28/99 0.30
09/29/99 0.10
09/30/99 0.00
TOTAL 4.90
000 0 lf~
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I INNER TIER
DAILY FLOW
I SEPT.
I 1999 IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9
09101199 76 27 88 97 167 68 138 569 222
09102/99 75 25 76 99 108 88 133 558 217
I 09/03/99 70 24 66 103 47 78 118 505 6
09/04/99 78 25 67 115 o 87 133 573 o
09105/99 80 25 78 107 o 87 136 584 o
09/06/99 74 24 65 94 o 80 120 492 1
I 09/07/99 79 24 72 104 254 89 123 531 62
09/08/99 24 24 65 111 250 86 122 474 415
09/09199 8 23 60 100 250 75 108 422 551
09110199 66 26 67 108 246 75 100 399 512
I 09111199 76 26 66 105 265 85 115 582 577
09112199 74 26 70 88 264 83 110 665 553
09113199 71 24 64 57 244 93 101 644 515
I 09114199 71 7 63 74 281 101 104 661 548
09115199 70 30 62 94 269 99 100 628 546
09116199 65 24 58 78 217 92 94 623 513
09117199 70 25 67 64 205 93 89 74 3
I 09118199 73 25 72 82 230 105 100 o o
09119199 70 24 72 75 236 104 101 o o
09120199 71 26 72 72 148 102 106 o 408
09121199 66 23 62 53 280 90 99 ,, 548
I 09122199 69 25 65 33 256 88 103 o 567
09123199 73 24 67 69 247 84 103 o 570
09124199 69 22 65 83 215 74 99 569 533
09125199 67 19 59 56 219 67 95 388 519
I 09126199 71 25 63 64 254 77 109 383 320
09127199 69 24 67 84 251 75 100 423 3
09128199 68 23 74 63 250 75 100 422 o
09129199 67 23 73 48 259 83 101 427 o
I 09130199 71 24 74 40 257 40 102 437 o
I AVG: 68 24 68 81 206 84 109 401 290
TOTAL: 2031 716 2039 2420 6169 2523 3262 12044 8709
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I 00001'7
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
ACTION
DATE WELL# PROBLEM DATE ACTION
9/1/99 #6 LOW FLOW 9/1/99 CHANGED METER & BLADDER
9/2/99 #3 LOW FLOW 9/2/99 ADJUSTED CONTROLS
9/2/99 #4 LOW FLOW 9/2/99 CHANGED AIR CONTROL VALVE
9/2/99 #5 LOW FLOW 9/2/99 CHANGED EXHAUSTER &METER
9/3/99 #1 LOW FLOW 9/3/99 ADJUSTED CONTROLS
9/7/99 #5 NO FLOW 9n199 REPLACED PUMP
9n199 #9 NO FLOW 9nt99 CLEANED SCREENS & PROBES
9/10/99 #1 LOW FLOW 9/10/99 REPLACED PUMP
9/19/99 #8 NO FLOW 9/19/99 REPLACED PUMP & EXHUSTER
9/19/99 #9 NO FLOW 09/19/99 RESET PUMP
000018
MECHANIC
P.P.
P.P
P.P.
P.P.
P.P.
P.P.
P.P.
P.P.
P.P.
P.P.
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0
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I DAILY REFERENCE SHEET:
I DATE: IT. EQ. PLT. DEC. DEC. WAS MIX MIX MIX NIT PHOS MIX F/M
SEPT. INF. TNK. SEP. LIQ LIQ LIQ ADD ADD LIQ WAS 5/DAY
1999 COD. COD. COD. COD. TSS. TSS MLSS NIT PHOS GALS LBS SET. GALS F/M AVG.
I 4380 3740 3880 105 32 2210 1532 128 5.2 2 140 135 0.23
2 4950 3780 9690 1612 106 13.6 1 2 140 135 0.00
3 4470 3810 3300 125 28 9000 1420 121 24.0 0 0 140 135 0.21
4 6220 4460 4650 98 28 3580 1496 167 32.0 0 0 150 80 0.28
I 5 8760 5260 1620 150 18.2 0 0 150 0 0.00 0.14
6 8240 5950 4920 100 20 8280 1588 140 22.0 1 1 140 120 0.28 0.15
7 7520 6610 8060 1532 97 14.8 1 2 140 135 0.00 0.15
8 7320 5840 5350 123 4 10480 1508 112 25.3 0 0 130 135 0.32 0.17
9 4820 4710 8400 1408 112 14.4 1 2 130 135 0.00 0.12 I 10 4910 4820 6040 122 16 8310 1568 130 26.0 0 0 100 135 0.34 0.19
11 5150 4100 5020 120 36 12900 1284 116 14.0 1 2 100 135 0.35 0.20
12 4580 4070 4160 1696 122 16.4 2 110 135 0.00 0.20
13 4650 4080 3730 118 8 9120 1724 117 16.0 2 110 100 0.19 0.18
I 14 4700 3940 4020 110 24 9700 1572 160 20.0 0 2 110 100 0.23 0.22
15 5300 3760 3840 131 40 11760 1480 128 28.5 0 0 110 100 0.23 0.20
16 3390 3230 7870 1640 111 8.0 1 2 110 100 0.00 0.13
17 4070 3730 2730 132 20 9910 1636 131 25.2 0 0 110 100 0.15 0.16
18 10850 4850 7010 1600 103 17.0 0 0 110 100 0.00 0.12 I 19 9910 6310 3940 120 48 10490 1620 101 19.0 0 110 100 0.22 0.12
20 10900 4980 10540 1444 108 12.0 2 110 100 0.00 0.07
21 3570 5790 4020 146 40 972 118 23.0 0 100 0 0.37 0.15
22 4280 4300 1768 122 12.0 2 110 100 0.00 0.12
I 23 4690 4050 4650 150 52 11500 1144 135 20.0 0 0 110 100 0.36 0.19
24 4930 4690 1500 167 16.0 0 0 110 0 0.00 0.15
25 3090 3950 2950 127 40 8180 1476 172 16.0 0 0 110 54 0.18 0.18
26 4470 3490 1416 141 10.0 1 1 110 0 0.00 0.11
27 7230 4370 3770 127 20 13100 1544 163 12.0 0 2 110 100 0.22 0.15 I 28 5890 4310 10550 1560 117 19.4 0 2 110 100 0.00 0.08
29 7020 4230 4170 143 76 6200 1692 116 21.6 2 110 100 0.22 0.12
30 6510 4600 16190 1440 144 19.6 0 2 110 100 0.00 0.09
31 #OIV/01 #DIV/01
I AVG: 5892 4527 3943 117 30 9088 1516 128.5 18.0 1 118 96 #DIV/01
MAX: 10900 6610 6040 150 76 16190 1768 172.0 32.0 1 2 150 135 #DIVf0I
MIN: 3090 3230 0 0 0 2210 972 97.0 5.2 0 0 100 0 #OIV/01
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GROUNDWATER MONTHLY MONITORING:
INNER TIER COMBINED INFLUENT #2 ITCI SBR MIXED LIQUOR: SBRML
PAGE N0.1 PAGE NO. 4
SEPT.1999 SEPT.1999 SETT. SLUDGE SIDAY
DATE· FLOW. PH: COD: TSS: TOC: DATE: PH: NH3N: "°"' oo, MLSS: MLVSS: SOLIDS: WASTED F/M: F/M:
GPO pH ppm ppm ppm pH ppm ppm ppm ppm ppm mo ,. '"'° ratio
09/01199 1452 , .. <380 10 1240 09,{>1/99 8.1 "' 5.2 3.5 1532 ,<O "' 0.23
09102/99 1379 , .. '950 10 09/02/99 8.2 HIB 13.8 3.5 1812 ,<O '35 0.00
09/03199 1017 , .. «70 11 09/03199 8.2 12' 24.0 3.3 "20 0.21
09/04199 1078 5.1 8220 8 09,0,199 8.1 "' 32.0 3.2 1498 150 80 0.28
09105/99 1097 5.2 8760 " 09/05'99 8.7 150 16.2 8.7 1820 150 0 0.00 0.14
09/06199 950 5.2 8240 8 09/08/99 8.8 "' 22.0 8.5 1586 "0 120 0.28 0"
09/07199 1338 52 7520 30 09/07/99 8.8 97 "8 8.2 1532 000 0.15
09/08199 1571 5.3 7320 " 2130 09/08199 8.7 "' 25.3 3.5 1502 1172 130 '35 0.32 0.17
0""9199 1597 5.3 4820 16 09/09'99 8.2 "' "' 3.7 "°' '30 "' 0.00 0.12
09/10/99 1599 5.3 4910 20 09110/99 82 130 26.0 ,.1 1568 100 '35 0.3' 0.19
09J11/99 1897 , .. 5150 " 09/11199 8.2 118 14.0 3.1 "" 100 "' 0.35 020
09/12/99 1933 ,., ,sao " 0,,12/99 8.2 '22 16.4 2.8 1698 110 '35 000 0.20
09/131'99 1813 5.3 ,aso 11 09/13199 8.2 m 16.0 3.2 1724 110 100 0.19 0.18
09/14199 1910 53 '700 20 09/14199 8.3 '80 20.0 2.8 '572 "" 110 100 0.23 0.22
09115/99 1898 5.3 5300 " 1530 09/15199 8.1 '28 28.5 2.7 "80 110 100 0.23 0.20
09J16/99 "" SA 3390 16 09/16199 8.1 "' 8.0 3A 18'0 110 100 000 0.13
09/17199 890 5.3 4070 " 09/17/99 8.2 "' 25.2 3.8 "" 1Hl 100 0.15 0.16
09118/99 887 5.1 10850 24 09118/99 8.1 103 17.0 3.7 '800 no 100 000 0.12
09119199 882 5.1 9910 14 09119/99 8.1 101 19.0 3., 1820 110 100 0.22 0.12
09120199 1105 5.1 10900 8 09/20/99 8.1 108 12.0 3.0 14« 110 100 0.00 0.07 0 09121/99 1232 5.2 3570 ' 09/21/99 8.1 "' 23.0 ,., 972 824 100 0 0.37 0.15
0 09122199 '208 52 4280 11 09/22'99 8.0 '22 12.0 3.8 1788 110 100 0.00 0.12
09123199 1237 5.2 '690 7 1410 09/23199 8.1 '35 20.0 3.9 11« 1,0 100 0.36 0.19
0 09/24/99 1729 5.1 4930 5 09/2<199 8.0 '87 18.0 ,.. 1500 110 0 0.00 0.15
09/25199 1489 5. 1 3090 09/25199 8.2 172 18.0 3.2 1476 100 " 0.16 0.18 0 09/"'99 1388 5.3 «70 ' 09/2""9 8.1 1" 10.0 ,.. 1418 110 0 0.00 0.11 rv 09/27199 1098 5.2 7230 8 09/27/99 8.1 '83 12.0 3.1 15'< 110 100 0.22 0.15
09/28/99 1075 5.2 5890 3 09/28199 8.1 m 19.4 2.8 1580 1272 110 100 000 0.08 ,:=) 09/29199 1081 5.2 7020 H) 2210 09129'99 8.1 "' 21.6 3.3 "" 110 100 0.22 0.12
09!30199 '°'' 5.2 8510 ' 09~0/99 8.1 1« 19.6 3.3 1«0 110 100 0.00 0.09
AVG· 1334 5.2 5892 14 "''' AVG 8.2 128 18 ' 1518 1131 116 93 0.14 0,15
MAX: 1933 SA 10900 " 2210 MAX: 8.8 172 32 7 1788 1272 150 135 0.37 022
MIN· 882 51 3090 3 1240 MIN· 8.0 97 5 3 972 82' 100 0 0.00 0.07
- - -- - - ---- -- --- ----
- - - ---- - ------- - ---
GROUNDWATER MONTHLY MONITORING· GROUNDWATER MONTHLY MONITORING·
AFTER PLATE SEPARATOR BEFORE SBR: SBRI SBR EFFLUENT:(OECANT) #4SBRE
PAGE NO. 3 PAGE NO. 5
SEPT.1999 SEPT.1999 WAS. NH3N PHOS.
DATE: PH COD: TSS: DATE: FLOW. COO: TSS:TSS ADDEO: ADDED: pH ppm ppm GPO ppm ppm ppm •" '"
09/01/99 5.< 3880 12 09/01199 2288 105 32 2210 2
09ro2199 09ro2199 0 9090 1 2
09ro3199 5.3 3300 8 09.<)3199 1875 125 28 9000 0 0
09"""9 8.0 -20 09"4'99 2474 88 28 3580 0 0
09ro5'99 09ro5'99 0 0
09/06/99 5.9 '920 32 09.<lS'99 2408 100 20 8280 1
09/07/99 09/07/99 0 8000 2
09/06/99 5.3 5350 8 o,ro8199 1918 123 ' 10'80 0 0
09""'99 09"""99 0 """' 1 2
09110/99 5.3 80<0 4 09/10'99 1899 122 1' 8310 0 0
09111/99 5.5 5020 12 09/11199 2438 120 38 12900 2 09112/99 09/12199 0 4160 1
09113/99 5.3 3730 4 0,,13'99 2019 118 8 9120 1 2
09114199 5.6 4020 8 09114'99 1908 110 24 9700 0 2
09/15199 5.6 3840 6 09/15199 2825 131 40 11760 0 0
09/Hl/99 09/18199 0 7870 1 2
09117199 5.7 2730 4 09117199 1875 132 20 9910 0 0
09118199 09118/99 7010 0 0
0 09119199 5.2 3940 12 09/19199 2298 120 46 10490 0
0 09120/99 09120'99 0 1054-0 2
09121199 5.3 4020 20 09121/99 2069 148 40 0 0 09122/99 oom'99 0 1 2
0 09123/99 6.2 4850 4 09123199 1879 150 52 11500 0 0
09124'99 09124'99 0 0 0
N 09125'99 5.9 2950 32 09125'99 24'6 127 40 8180 0 0
09126199 09128199 0 1 ,.... 09!27199 5.3 3770 4 09fl.7/99 2825 120 20 13100 0 2
09128/99 09128199 0 10550 0 2
09129"' 5.2 4170 40 09128199 2325 143 76 6200 1 2
09/30/99 09130'99 0 16190 0 2
AVG· 5.5 4175 14 AVG: 1337 123 31 9088 1
MA>C 6.2 80<0 40 MAX: 2825 150 78 16190 2
MIN 5.2 2730 4 MIN: 0 96 4 2210 0 0
010 NOT PROCESS SBR.
GROUNDWATER MONTHLY MONITORING: GROUNDWATER MONTHLY MONITORING
INNER TIER EQUALIZATION TANK: ITEQT INNER TIER CARBON FILTER EFFLUENT 18 ITEF PAGE N0.2 PAGE NO. 7
SEPT.1999 SEPT.1999
DATE: PH· COO: OTWATERADDED DATE· PH: COD: TOC: TSS: pH ppm ,., pH ppm ppm ppm
09/01/99 7.4 3740 563 09/01/99 8.2 101 7 24 09,02199 7.4 3780 09,<)2199
09/03/99 7.3 3810 09,03'119
09"'4"'9 7.1 "''° 09/04199
09,05"'9 7.8 5250 09,0"'9
09,0099 7.3 5950 375 og,oogg
09/07/99 7.3 8610 09,{17/99
09,08/ll9 7.4 5840 375 09,08/99 8.5 102 8 09,09'99 7.4 4710 09,<)8/99
09110/99 7.3 '820 09110/99
09111/99 7.5 4100 450 09111/99
09/12199 7.5 4070 09/12199
09113199 7.3 4080 09113199
09114/99 7.3 3940 375 09114199
09/15199 7.4 3780 863 09115199 8.2 131 8 09116199 7.4 3230 09116199
09117199 7.2 3730 09117199
0 09118/99 7.4 4850 09118/99
09/19/99 7.4 8310 450 09119199 0 09n0"'9 7.4 4980 09a0/99
0 09121/99 7.2 5790 09121/99 09mm 7.2 4300 09a2/99 0 09n:3'99 7.2 4050 09a3199 8.3 138 ' N 09/24199 7.3 4690 09/24199
09n5"'9 7.3 3950 09n5199
N 09n8199 7.2 3'90 09a8199
09/27199 72 4370 09127199
09n8/ll9 7.2 4310 09n"'99
09n9'99 7.3 '230 09n9199 8.2 137 8 09/30/99 7A '800 0900'99
AVG. 7.3 4527 450 AVG: 8.3 122 7 24 MAX: 7.8 8610 863 MAX: 8.5 138 8 24 MIN: 7.1 3230 375 MIN: 8.2 101 4 24
- - -- ----- - --- - -----
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GROUNDWATER MONTHLY MONITORING:
RAINFALL DATA
DATE INCHES/DAY
10/01/99 o.oo
10/02/99 0.00
10/03/99 0.00
10/04/99 0.70
10/05/99 0.00
10/06/99 0.00
10/07/99 0.00
10/08/99 o.oo
10/09/99 0.05
10/10/99 4.60
10/11/99 0.00
10/12/99 0.00
10/13/99 0.10
10/ 14 /99 0.00
10/15/99 0.00
10/16/99 o.oo
10/17/99 0.00
10/18/99 0.00
10/19/99 0.10
10/20/99 0.50
10/21/99 0.00
10/22/99 0.00
10/23/99 0.00
10/24/99 0.00
10/25/99 0.00
10/26/99 0.00
10/27/99 0.00
10/28/99 0.00
10/29/99 o.oo
10/30/99 0.00
10/31/99 0.00
TOTAL 6.05
000023
I
INNER TIER I DAILY FLOW
OCT. I
1999 IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9
10/01/99 69 24 71 38 268 29 101 431 4 I
10/02/99 66 23 69 39 267 28 101 431 0
10/03/99 65 23 71 34 243 25 96 433 0
10/04/99 67 23 67 32 254 24 95 441 8 I 10/05/99 57 21 63 47 242 n 96 442 9
10/06/99 53 22 69 58 245 92 94 448 8
10/07/99 51 23 59 62 263 91 94 443 0
10/08/99 53 22 55 67 285 92 93 459 8 I 10/09/99 52 23 55 64 275 92 96 463 0
10/10/99 72 22 191 335 253 87 90 447 0
10/11/99 53 22 135 184 272 89 94 467 0 I 10/12/99 50 22 65 65 281 90 96 469 0
10/13/99 50 22 60 57 262 90 96 467 0
10/14/99 50 22 63 57 278 91 98 476 21
10/15/99 49 23 63 60 278 94 101 485 0 I 10/16/99 51 23 65 59 282 95 105 500 0
10/17/99 48 21 60 56 286 90 104 445 0
10/18/99 50 22 59 59 299 94 · 105 481 507
10/19/99 51 22 65 61 298 94 103 421 668 I 10120/99 50 21 61 60 288 90 101 231 613
10/21199 52 22 60 58 326 93 107 227 589
10/22199 53 22 59 61 300 93 104 224 638
10/23/99 37 16 43 44 223 67 78 196 419 I 10/24/99 50 24 63 62 279 77 91 245 523
10/25/99 40 17 46 51 233 62 79 36 523
10/26/99 51 23 65 63 294 74 91 441 618
10/27/99 52 0 68 69 334 76 109 453 680 I 10/28/99 45 29 53 56 287 67 82 366 579
10/29/99 53 26 68 74 267 71 87 387 571
10/30/99 57 24 69 70 287 87 104 509 665
0/31/99 53 22 65 68 284 84 103 523 608 I
,VG: 53 22 69 70 275 78 97 403 266 I rAL: 1650 671 2125 2170 8533 · 2405 2994 12487 8259
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MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
ACTION
DATE WELL# PROBLEM DATE ACTION
10/4/99 #4 LOW FLOW 10/4/99 REPLACED BLADDER
10/4/99 #6 LOW FLOW 10/4/99 REPLACED BLADDER
10/8/99 #9 NO FLOW 10/8/99 CLEANED PROBES & SCREEN
10/18/99 #9 LOW FLOW 10/18/99 RESET PUMP & RESET FLOW RATE
10/26/99 #8 LOW FLOW 10/26/99 REPLACED EXHUSTER
10/28/99 #2 NO FLOW 10/28/99 ADJUSTED PUMP & SET FLOW RATE
000025
MECHANIC
P.P.
P.P.
P.P.
P.P.
P.P.
P.P.
=:,
..::> a
0
i\) ,:n
Well
OT-2R
OT-3
OT-4
OT-5
OT-6
OT-6A
OT-7
OT-8
Thermometer
Operational? ..
X
X
X
X
X
X
X
X
Monthly O&M Plan Checklist
HNA Holdings, Inc., Shelby, NC
Heat Lamp
Operational?·,...
X
X
X
X
X
X
X
X
Other Operational Items/Comments
changed bulb
(.. Temperature and Heat Lamp checks October thru April only)
Form Completed by: __________ T.c:OecNYC!..!...~B~R.!.YANT=.!_ ________ _
Date: ___________ 1.:...0"'/'-'1'-'/-"9-"9 __________ _
-------------------
--- ------ - - --- - - ---Quarterly O&M Plan Checklist-HNA Holdings, lnc./Shelby, NC Form Completed by: TONY BRYANT
Date: 10/1/99
Open Sample Energize Verify De-energize Close Sample Varity HHtar Secure Wall
Port Pume Discharge Pump Port oeeratlon Vault Comments
Outer Tier Well
OT-2R X X X X X X X
OT-3 X X X X X X X
OT-4 X X X X X X X
0 OT-5 X X X X X X X
0
0 OT-6 X X 0 X X X X X
1'v
""1 OT-6A X X X X X X X
OT-7 X X X X X X X
OT-8 X X X X X X X
;,·-:,-;"
Energize Energize Energize Energize Enuglze
Ground-Water AS Blower Transfer Pump Transfer Pump Transfer Pump Transfer Pump
Treatment Sys. Y-V-1008 Y•P•1007A Y-P-10078 Y-P-1008A Y•P•100BB Comments
I
DAILY REFERENCE SHEET: I
DATE: IT. EQ. PLT. DEC. DEC. WAS MIX MIX MIX NIT PHOS MIX F/M I OCT. INF. TNK. SEP. LIQ LIQ LIQ ADD ADD LIQ WAS 5/DAY
1999 COD. COD. COD. COD. TSS. TSS MLSS NIT PHOS GALS LBS SET. GALS F/M AVG.
1 6910 4780 5620 239 20 8660 2004 131 31.3 0 0 110 100 0.25 I 2 5680 4310 10120 1792 116 21.0 0 100 100 0.00
3 6660 5160 4740 134 52 2630 1484 103 22.8 1 100 100 0.28
4 6520 4750 1668 131 21.1 0 0 100 100 0.00
5 6550 5710 964 121 20.0 0 0 100 100 0.00 0.11 I 6 5760 5130 4400 90 32 10160 1612 109 20.2 2 100 100 0.24 0,11
7 5240 4940 8900 1632 139 19.6 0 0 100 100 0.00 0.11
8 5810 5320 5270 150 40 5460 1942 132 20.1 0 0 100 100 0.24 0.10
9 6800 6090 12100 1644 103 15.6 0 0 100 100 0.00 0.10
10 5790 6070 5490 186 16 1168 117 14.3 1 1 90 0 0.42 0.18 I 11 4850 3820 13670 1532 118 15,6 1 2 100 100 0.00 0.13
12 5940 3800 4960 159 48 9550 1492 150 24.0 0 0 100 100 0.30 0.19
13 6090 4530 10130 1500 130 20.2 0 0 100 100 0.00 0.14
14 6870 4580 4170 205 28 9980 1576 133 20.2 0 0 50 100 0.24 0.19 I 15 6890 5440 10920 1580 107 16.2 1 1 100 100 0.00 0.11
16 7370 5860 5120 190 88 10620 1336 111 22.5 1 1 100 100 0.34 0.17
17 6920 4800 1268 140 25.0 0 0 100 0 0.00 0.12
18 7310 4730 4830 192 80 8560 980 118 22.8 0 0 100 100 0.44 0.20
19 3500 455 10100 1576 124 11.8 0 2 80 100 0.00 0.16 I 20 3600 3770 5160 179 60 7230 1176 112 27.2 0 0 70 100 0.39 0.23
21 3740 3910 10670 1016 113 14.4 0 2 70 100 0.00 0.17
22 4040 4080 3750 186 80 10720 1368 82 28.0 1 1 70 100 0.24 0.21
23 3420 3210 12530 1348 103 21.5 0 0 70 100 0.00 0.13 I 24 4270 3400 3820 201 40 3060 1412 88 20.2 1 70 100 0.24 0.17
25 4100 3610 13200 1128 118 18,0 0 0 70 100 0.00 0.10
26 4220 3930 3580 255 80 10090 1404 127 16.5 0 2 70 100 0.23 0.14
27 3870 3830 3950 242 92 10490 1492 89 23.7 0 70 100 0.24 0.14
28 3530 3160 11580 1256 114 14.8 2 50 100 0.00 0.14 I 29 4430 4030 3440 225 72 13920 924 125 26.5 0 0 50 100 0.33 0,16
30 4140 3580 3770 224 88 12000 1440 100 26.2 0 100 100 0.23 0.21
31 4290 3940 3480 226 72 12000 1408 100 15.0 0 0 100 100 0.22 0.20
AVG: 5326 4346 4197 182 55 9965 1423 116.3 20.5 0 87 94 0.16 I MAX: 7370 6090 5620 255 92 13920 2004 150.0 31.3 1 2 110 100 0.44
MIN: 3420 455 0 0 0 2630 924 82.0 11.8 0 0 50 0 0.00
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-- - ---- - --- ---- - -- -GROUNDWATER MONTHLY MONITORING: INNER TIER COMBINED INFLUENT #2ITCI SBR MIXED LIQUOR: SBRML PAGEN0.1 PAGE NO. 4 OCT,1999 OCT.1999 SETT. SLUDGE 5/DAY DATE: FLOW. PH: COO: TSS: TOC: DATE: PH, NH3N: "°'' ro MLSS: MLVSS: SOLIDS: WASTED F/M: F/M: GPO pH ppm ppm ppm pH ppm ppm ppm ppm ppm m" ,,, ratio ratio 1001199 1035 5.2 6910 15 10/01/99 8.1 131 31.3 3.1 2004 110 100 0,25 10/02199 1024 5.2 5880 1 10/02199 8.1 118 21.0 0.0 1782 100 100 0.00 1003/99 990 5.2 8860 5 1Ml3/99 8.1 103 22.8 3.6 1464 100 100 0.28 10/04199 1011 5.2 6520 4 1""4199 ·s.2 131 21.1 3.6 1666 100 100 0.00 10/05/99 1054 5.0 8550 5 1005199 8.2 121 20.0 .., 964 824 100 100 0.00 0.11 1005/99 1089 5.0 57ll0 8 2050 1"""99 8.3 109 20.2 42 1812 100 100 0.24 0.11 10/07/99 1088 5.1 5240 8 10/07/99 8.2 139 1s.e •. , 1032 100 100 000 0.11 10/08/99 11>4 5.2 5810 10 1""8199 82 132 20.1 ,.1 1942 100 100 0.2-1 0.10 10,00/99 1120 5.1 8800 10 10/09'99 8.1 103 15.8 4.4 1844 100 100 0.00 0.10 10/10/99 1497 52 5790 7 10/10199 8.1 117 14.3 •• 1188 90 0 0.42 0.18 10111199 1318 51 4850 " 10/11199 8.2 118 15.8 •• 1532 100 100 0.00 0.13 10/12'99 1138 5.2 5940 12 10/12/99 8.3 150 24.0 4< 1492 1152 100 100 0.30 0.19 10/13199 1104 5.1 8090 5 10/13199 8.1 130 20.2 3.9 1500 100 100 0.00 0.1◄ 10/14/99 1158 51 6870 6 1980 10/1""99 6.1 133 20.2 3.7 157& 50 100 0.24 0.19 10/15/99 1153 51 6890 4 10/15199 8.1 107 16.2 1.6 1580 100 100 0.00 0.11 10/16.-99 1180 5.1 7370 11 10/18199 8.1 111 22.5 3.1 1330 100 100 0.>4 0.17 10117199 1110 5., 0920 52 10/17199 8.1 140 25.0 3.6 1208 100 0 000 0.12 ·10/181<.l9 1676 5.1 7310 15 10118199 6.2 116 22.0 3.4 960 100 ,oo 0.44 0.20 1CY19/99 1704 5.2 3500 10 10/19.'99 8.1 124 11.8 3.4 157ll 1218 80 100 0.00 0.16 0 10(2Q/99 1515 5.3 3600 4 1180 1"20/99 8.1 112 27.2 3.7 1176 70 100 0.39 0.23 10/21199 1534 5.2 3740 10 10121/99 81 113 14.4 2.9 1016 70 100 0.00 0.17 0 1(Y22,09 1554 5.2 4040 13 1"22199 8.0 62 28.0 3.9 1368 70 100 0.24 0.21 0 10/23199 1123 5.2 3420 8 1"23199 8.1 103 21.5 3.4 1346 70 100 000 0.13 1CY24/99 1414 53 4270 "' 1"2<199 8.1 88 20.2 0.7 1412 70 100 0.24 0.17 0 10/25199 1067 5.2 4100 "' 1"25199 8.1 116 18.0 0.5 1128 70 100 0.00 0.10 "'""" 1720 5.1 4220 7 1"28199 6.7 "' 16.5 8.0 140< 1118 70 100 0.23 0.14 l'\) 10'27199 104, 5.3 3670 10 1180 10/27199 0.5 .. 23.7 7.7 1492 70 100 0.24 0.14 c;, 10/28/99 1564 54 3530 11 1"26199 8.2 114 14.8 3.7 1256 50 100 0.00 0.14 10f29/99 1604 5.3 4430 20 1"28199 8.1 125 26.5 4.7 924 50 100 0.33 0.16 10/30/99 1872 5.3 4140 7 10/30/99 8.0 100 26.2 3.1 1440 100 100 0.23 0.21 10131/99 1810 5.3 4290 5 1001/99 8.0 101 15.0 2.8 1408 100 100 AVG: 1332 5.2 5326 11 1593 AVG: 62 116 21 4 1423 1on 87 94 0.15 0.15 MAX 1872 5.4 7370 52 2050 MA>C 8.7 150 31 ' 2004 1218 110 100 0,44 0.23 MIN· 890 5.0 3420 1 1160 MIN: 8.0 82 12 0 "' 824 50 0 0.00 0.10
GROUNDWATER MONTHLY MONITORING: GROUNDWATER MONTHLY MONITORING:
AFTER PV.. TE SE PARA TOR BEFORE $BR: SBRI SBR EFFLUENT:(DECANl) #4SBRE PAGE NO. 3 PAGE NO. 5
OCT.1999 OCT.1999 WAS. NH3N PHOS
DATE: PH: COD: TSS: DATE: FLOW. COD: TSS:TSS ADDED. ADDED: pH pPm ppm GPO pPm ppm p,m ,., ,.,.
10/01/99 5.4 5620 10/01/99 2301 239 20.0 8660 0 D 10,02/99 10,02199 0 10120 0 10/03/99 5.6 4740 40 10,03199 1838 '34 52 2830 1 1"""'9 "'"""" 0 0 D 10/05199 10,0"98 0 0 D 1""'99 5.4 '400 4 lM>e/99 2031 80 32.0 10160 1 2 10/07/99 1M7199 0 8800 0 0 10/08/99 59 5270 28 10,08/99 2292 150 40 5460 0 D 10/09199 10,09'99 0 12100 0 0 10/10199 59 5490 24 10/10199 1857 166 16 1 10/11/99 10/11199 0 13670 2 10/12199 5.4 4960 4 10/12/99 1875 159 48 9550 0 0 10/13/99 10/13199 0 10130 0 D 10/14/99 5.8 4170 8 10114199 2370 205 28 9980 0 0 10115/99 10/1.5199 0 10920
10/16199 5.8 5120 24 10/18/99 1998 180 86 10620 1 10/17/99 10/17199 0 0 D 10118/99 5.3 4830 8 10/18199 1731 192 80 8560 0 0
10/19/99 10/19199 0 10100 0 2 0 10/20'99 5.4 5180 12 10/20'99 1706 179 80 7230 0 0
0 10/21199 10/21/99 0 10670 0 2 10/22'99 5.5 3750 20 10/22'99 2536 166 80 10720 1
0 10/23/99_ 10/23199 0 12530 0 0 10/24199 5.4 3820 28 10/24/99 2'42 201 40 3060 1 0 10/25199 10l25'99 0 13200 D 0 w 10/28/99 6.4 3580 20 10'28/99 2250 255 80 10090 0 2 10/27199 " 3950 10/27199 2588 242 92 10490 0 Cl 10/28'99 10/28199 D 11580 1 2 10/29/99 5.4 3'40 10/29'99 2215 225 72 13920 0 D 10/30'99 ,.o mo 8 10,,c,99 2505 224 8B 12000 1 D 10/31/99 5.8 3480 4 10/31/99 2207 226 72 12000 0 0
AVG: 5.7 4'44 15 AVG: 1185 193 58 9985 0 1 MAX· 6.4 5620 40 MAX: 2588 255 92 13920 1 2 MIN 5.3 3'40 4 MIN: 0 90 18 2830 0 0
DID NOT PROCESS SBR.
--- - - --- ---- - --- - --
----- --- --- -- --- -- -
GROUNDWATER MONTHLY MONITORING: GROUNDWATER MONTHLY MON I TORIN'
INNER TIER EQUALIZATION TANK: ITEOT INNER TIER CARBON FILTER EFFLUENT #SITEF
PAGE NO. 2 PAGE NO. 7
OCT.1999 OCT.1999
DATE: PH: COD: OT WATER ADDEO DATE: PH: COD: TOC: TSS:
pH ppm ,., pH ppm ppm ppm
07/01197 7.3 4780 10/01/99
07/02197 7.3 4310 10/02/99
07/03197 7.2 5160 375 10/03/99
07/04197 7.5 4750 10""'99
07'05197 7.4 5710 10/05199
07/06/97 7.2 5130 1""""' 8.1 es 9 ,.
07/07/97 7.3 '940 1007/99
07/08/97 7.< 5320 375 10/08199
07/09/97 7.4 ,090 10"'9199
07/10/97 7.4 0070 10110/99
07111197 7.5 3820 10/11/99
07/12/97 7.5 3800 10/12199
07/13197 1., '530 10/13199
07114/97 7.4 '580 10/14/99 8.2 157 9
07115/97 1., 54'0 10/15/99
07/16197 7.5 58,0 338 10/1&'99
07117/97 7.5 4800 10/17/99
07118/97 7.5 4730 375 10/18199
07119197 1., '550 10/19199
07'20/97 7.4 3770 10120/99 8.3 17' 9
0 07121197 7.6 3910 10121/99
07122197 7.5 <080 1oml99 0 0712.3197 7.5 3210 10/23'99
0 07'1.4197 7.6 3'00 10/2"99
07125197 7.5 3810 10/25'99 0 07128197 7.5 3930 10126199 w 07f1.7/97 7.5 3830 163 10127/99 6.5 220 10
0712.8197 7.6 3160 10/28199 ...... 07129/97 7.4 <030 10/29/99
07130/97 7.7 3580 10'30/99
07'31197 7.6 39<0 486 10/31/99
AVG 7.4 «76 358 AVG: 63 159 9 24
MAX 7.7 ,090 .... MAX, 6.5 220 10 24
MIN: 7.2 3160 163 MIN: 6.1 es 9 24
GROUNDWATER MONTHLY MONITORING:
RAINFALL DATA
NOV 1999 .
DATE INCHES/DAY
11/01/99 0.70
11/02/99 o.oo
11/03/99 0.00
11/04/99 0.00
11/05/99 0.00
11/06/99 0.00
11/07 /99 0.00
11/08/99 o.oo
11/09/99 0.00
11/10/99 0.00
11/11/99 0.00
11/12/99 0.00
11/13/99 0.00
11/14/99 0.00
11/15/99 0.00
11/16/99 0.00
11/17/99 0.00
11/18/99 0.00
11/19/99 0.00
11/20/99 o.oo
11/21/99 0.00
11/22/99 0.00
11/23/99 0.00
11/24/99 o.oo
11/25/99 0.90
11/26/99 0.05
11/27 /99 0.00
11/28/99 0.00
11/29/99 0.00
11/30/99 0.00
TOTAL 1. 65
000032
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I INNER TIER
DAILY FLOW
I NOV.
1999 IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9
I 11101/99 45 19 58 58 248 70 87 428 511
11102199 53 22 66 59 279 74 95 440 570
I 11103199 53 14 67 69 315 82 114 495 645
11104/99 49 22 62 68 294 79 104 454 601
11105199 53 23 69 80 291 81 112 457 624
11106199 56 23 78 73 319 86 120 467 721
I 11107199 52 20 80 74 292 81 111 438 661
11108199 37 18 76 71 237 75 109 406 593
11109199 52 21 79 69 238 75 100 389 619
11110199 55 22 84 75 259 81 109 438 655
I 11111/99 55 22 86 77 278 80 86 343 662
11/12/99 54 23 80 80 290 79 32 280 620
11113199 55 23 86 83 302 76 29 378 632
11114199 56 22 87 88 293 77 30 388 678
I 11115/99 56 22 88 91 278 81 30 370 674
11/16/99 54 22 86 97 264 79 120 343 637
11/17/99 47 22 81 92 254 . 67 140 ·290 480
11110/99 48 23 79 89 246 81 135 265 354 I 11119199 49 24 78 90 246 75 129 262 460
11120199 52 16 81 97 265 73 149 297 500
11121/99 53 17 83. 90 272 74 147 302 501
11122/99 53 24 82 93 221 70 142 300 491 I 11123/99 53 26 82 88 212 70 140 309 481
11/24/99 53 21 84 96 219 70 140 259 417
11125/99 53 21 82 93 217 68 138 237 433
11/26199 55 21 87 104 231 69 143 300 480 I 11127/9~ 49 19 79 80 213 62 131 343 475
11128191 49 20 81 85 228 62 128 378 477
11/29191 51 22 87 89 217 64 135 410 500
I 11/3019\ 47 21 84 89 217 64 137 409 499
I AVG: 52 21 79 83 258 74 111 363 555
iOiAI 1547 635 2382 2487 7735 2225 3322 10875 16651
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MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
ACTION
DATE WELL# PROBLEM DATE ACTION
11/16/99 #7 LOW FLOW 11/16/99 REPLACED BLADDER
11/18/99 #9 LOW FLOW 11/18/99 REPLACED METER &CLEANED PROBES
000034
MECHANIC
P.P.
P.P.
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-------------------
0
0
0 :::,
w
-:,;1
Well
OT-2R
OT-3
OT-4
OT-5
OT-6
OT-6A
OT-7
OT-8
Thermometer
Operational? ..
X
X
X
X
X
X
X
X
Monthly O&M Plan Checklist
HNA Holdings, Inc., Shelby, NC
Heat Lamp
Operational? ..
X
X
X
X
X
X
X
X
Other Operational Items/Comments
('"' Temperature and Heat Lamp checks October thru April only)
Form Completed by: ----------'-TO=NY.:....::Bc:.cRc:.Yc.:ANT=----------
Date: 11/1/99 ---------~~~~---------
I
DAILY REFERENCE SHEET: I
DATE: IT. EQ. PLT. DEC. DEC. WAS MIX MIX MIX NIT PHOS MIX F/M I NOV. INF. TNK. SEP. LIQ LIQ LIQ ADD ADD LIQ WAS 5/DAY
1999 COD. COD. COD. COD. TSS. TSS MLSS NIT PHOS GALS LBS SET. GALS F/M AVG.
4920 3230 8090 1564 119 8.0 0 2 70 100 0.00 I 2 3890 2980 3180 181 76 9880 1424 120 17.0 2 70 100 0.20
3 4150 4290 3610 218 76 13230 1372 100 20.3 2 70 100 0.23
4 4410 3630 9890 988 110 23.2 0 0 70 100 0.00 I
5 4050 3520 3040 206 72 5600 1484 106 18.6 1 2 70 100 0.18 0.12 I I 6 4580 3960 3580 212 64 14110 1416 120 26.0 0 0 60 100 0.22 0.17
7 3960 3220 3140 180 72 6360 1224 110 22.6 0 0 50 100 0.23 0.17
8 3550 3910 16820 1076 102 11.3 1 2 50 100 0.00 0.13
9 3160 3100 3460 202 76 2230 1120 125 17.0 0 2 50 100 0.27 0.18
10 3410 3270 4360 167 48 9570 1348 115 19.5 2 50 100 0.29 0.20 I 11 3910 3760 10670 1548 141 18.5 0 0 50 100 0.00 0.16
12 4550 4380 3680 153 4 15820 1436 117 19.6 1 2 50 100 0.23 0.16
13 4180 3360 3430 163 72 8260 1620 120 22.0 0 0 50 100 0.19 0.20
14 3860 3510 5160 1640 142 13.7 0 2 50 100 0.00 0.14 I 15 3820 3860 3270 132 20 9790 1424 119 21.8 1 2 50 100 0.20 0.12
16 5060 4450 3010 1388 130 20.0 0 0 50 100 0.00 0.12
17 4860 4060 3570 145 32 12230 1584 121 19.6 0 0 50 100 0.20 0.12
18 4170 3570 4000 146 20 2170 1552 114 13.0 2 50 100 0.23 0.13
19 4560 4330 1580 96 18.1 2 50 40 0.00 0.13 I 20 4860 4580 3990 155 28 2624 1384 104 28.6 1 0 50 100 0.26 0.14
21 3660 3590 1628 150 18.0 0 2 50 100 0.00 0.14
22 4380 4350 4970 211 40 14560 1072 120 23.2 0 0 50 100 0.41 0.18
23 3970 3140 1864 110 14.2 2 50 0 0.00 0.13 I 24 3460 3790 3940 135 20 4010 1008 113 25.6 0 0 50 50 0.35 0.20
25 4300 4080 1520 140 20.0 0 0 40 0 0.00 0.15
26 4400 4160 3860 139 24 2368 1436 116 12.0 2 40 40 0.24 0.20
27 5000 3970 1976 140 32.0 0 0 40 0 0.00 0.12
28 3900 3160 3630 124 40 2076 144 24.0 0 0 50 0 0.16 0.15 I 29 4990 4090 20690 1024 102 2.0 2 50 50 0.00 0.08
30 3690 3090 4370 139 16 12750 1224 144 23.6 0 0 50 40 0.32 0.14
#OIV/0! #OIV/01
I AVG: 4189 3746 3531 158 42 9162 1433 120.3 19.1 0 1 53 77 #OIV/01 I MAX: 5060 4580 4970 218 76 20690 2076 150.0 32.0 1 2 70 100 #OIV/01
MIN: 3160 2980 0 0 0 2170 988 96.0 2.0 0 0 40 0 #OIV/01
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000036 I
- -------- -- --- -- -- -GROUNDWATER MONTHLY MONITORING: INNER TIER COMBINED INFLUENT #2 ITCI SBR MIXED LIQUOR: SBRML PAGE NO.1 PAGE NO. 4 NOVEMB"'R 1999 NOVEMBER.1999 SETT SLUDGE 5/DAY DATE: FLOW. PH: COD: TSS TOC: DATE: PH, NH3N: ""' ro MLSS: MLVSS: SOLIDS: WASTED FIM: F/M: GPO pH ppm ppm ppm pH ppm ppm ppm ppm ppm m" ,,, -ratio 11/01/99 1524 5.3 4920 10 11/011'99 8.2 119 8.0 3.7 1564 7D ,oo D.00 ,i,omg 1658 52 3"0 5 11/02/99 8.0 ,20 17.0 •. , 1◄24 ,, .. 7D ,oo 0.20 11/03199 185< 5.3 4150 10 1100 11/03199 8.1 ,oo 20.3 3.7 1372 70 ,oo 0.23 11/04199 1733 5.3 «10 10 11I0</99 81 ,10 23.2 3.5 988 70 ,oo 000 11/05/99 1790 5.2 4050 13 11/05199 8, ,., 18.6 <.3 5000 70 ,oo 0.18 0.12 11/Q&W 1943 5.3 4580 , 11/06/89 8.1 ,20 28.0 3.8 14110 00 ,oo 0.22 0.17 11/07/99 1809 5.2 3960 8 11/07199 8.1 110 22.6 ,., ,,,. 50 ,oo 0.23 0,17 11/08,W 1622 5.2 3550 ' 11Kl8/99 8.0 102 11.3 5.2 1076 50 ,oo 000 0.13 11109/99 ,.., 5.2 3160 3 1160 ,,,,.,.. 80 125 17.0 5.5 1120 958 50 ,oo 0.27 0.18 11/101119 me 5.3 3'10 • 11/10/99 8.0 115 19.5 ,.3 ,,.. 50 ,oo 0.29 0.20 11/11199 "" 5.2 3910 5 11/11199 8.1 ,., 16.5 3.9 , ... 50 ,oo 000 0.16 11112199 1532 5.2 4550 7 11/12/99 8.0 ,,, ,s.e 5.1 ,.,. 50 ,oo 0.23 0.16 11113199 , ... 5.3 4180 7 11/13'99 ,, 120 22.0 3.7 1820 50 ,oo 0.19 0.20 11/14/S!I 1719 5.3 3800 3 11/14199 ', 142 13.7 3 .• "" 50 ,oo 0.00 0.14 11/15/99 1890 5.3 3820 , 11/15199 ,, ,,. 21.8 3.9 1424 50 ,oo 0.20 0.12 11/16199 1702 5.3 506C • 11/18199 81 130 20.0 •. 9 1388 1200 50 ,oo 0.00 0.12 11/17199 1473 5.3 ,eeo ,, ,,., 11/17/99 9.1 ,,, 19.e ,.1 ,,,. 50 ,oo 0.20 0.12 11118199 1320 5.3 4170 ' 11/16199 ,, ,,, 13.0 5.1 ,,,, 50 HJO 0.23 0.13 11/19199 1413 5.3 •seo ,. 11/19/99 81 98 18.1 55 1580 50 40 0.00 0.13 11/20/99 1530 5.2 ,eeo 33 11/20199 7.9 ,04 28.6 2.9 1394 50 ,oo 028 0.14 ,.=, 11/21199 1539 5.3 3600 13 11121199 8.0 ,so 18.0 •.3 1628 50 ,oo 0.00 0.14 ,,,,,,.,, 1476 5.2 '380 ' ,,,,,,., 8.0 120 23.2 ,.2 ,072 50 ,oo 0.41 C.18 0 11123/99 , .. , 5.3 3970 13 11123199 8.0 1,0 14.2 4.8 ,.,. ''°' 50 0 0.00 0.13 0 11124199 13S9 5.3 "'° ,,, 1350 11/24199 8.0 ,,, 258 8.2 1008 50 50 0.3S 020 11/25/99 13'2 5, 4300 20 11125199 ,., 1'0 20.0 ,., 1520 40 0 0.00 0.1S 0 ,,,,.,., 1'90 5.3 .. oo ,,, 11/28199 ,., ,,. 12.0 . , ,.,. 40 40 0.24 1l20 11/27199 14S1 51 5000 32 11127199 ,., 1'0 32.0 3.9 1976 40 0 0.00 0.12 w 11128/99 ,so, 52 3900 .. 11/28199 ', , .. 24.0 4.7 2076 50 0 0.16 0,15 --l 11129199 1S7S 5.3 '990 ,, 11129/99 ', 102 2.0 5.0 1024 50 0 000 0.08 11/30/99 1587 5.3 3690 ,, 11130/99 8.0 , .. 238 5.8 1224 1016 50 40 0.32 0.14 AVG: 1S9S 53 4189 22 124S AVG: 8.1 ,20 ,, • '"' ,,,. 53 78 0.15 0.1S MAX: 19<3 5.3 5000 ,,, 1350 MAX: 82 ,so 32 8 14110 ''°' 70 ,oo 0.41 0.20 MIN: 1320 5, 3160 , "" MIN; 7.9 98 2 , 988 958 40 0 000 0.08
GROUNDWATER MONTHLY MONITORING: GROUNDWATER MONTHLY MONITORING:
AFTER PLATE SEPARATOR BEFORE SBR: SBRl SBR EFFLUENT:(OECANT) #4 SBRE
PAGE NO. 3 PAGE NO. 5
NOVEMBER.1999 NOVEMBER.1999 WAS. NH3N PHOS.
DATE: PH: COD: TSS: DATE: FLOW: COD: TSS: TSS ADDED: ADDED: pH ppm ppm GPD ppm ppm ppm ,. '"
11/01/99 11/01199 0 8090 0 2
11/02/99 54 3180 11/02/99 2237 18\ 78 9880 2
11/03/99 5.7 3610 ' 11/03/99 2561 218 76 13230 1 2
11/04/99 11/04199 0 9890 0 0
11/05199 54 3040 ' 11/05199 2051 206 72 5600 1 2
11,oe,gg 54 3580 ' 11/0099 171-4 212 "' 1-4110 0 0
11/07/99 5.8 3140 18 11/07199 26<9 179 72 8360 0 0
11/08/99 11""'9 0 16820 1 2
11/09199 5.9 3460 12 11/09/99 2200 202 78 2230 0 2
11110/99 5.6 <360 ' 11/10{99 2025 167 48 9570 1 2
11111/99 11111199 0 10870 0 0
11/12/99 7.0 3690 • 11/12/99 2132 153 • 15820 1 2
11113/99 ,., 3'30 '° 11113199 2611 163 72 8260 0 0
11114/99 11/1-4/99 0 5180 0 2 11115199 5.3 3270 ' 11115199 2280 132 20 9790 1 2
11116199 11116199 0 3010 0 0
11117/99 54 3570 8 11117199 2391 1<5 32 12230 0 0
11116199 5.6 ,ooo 20 11118199 2'96 1'8 20 2170 2
0 11119/99 11119199 0 2
11120/99 6.6 3990 • 11/20{99 2108 155 28 2624 1 0
0 11121/99 11121199 0 0 2
11122/99 8.8 4970 18 11122199 2-402 211 '° 1'560 0 0 0 11/23/99 11123199 0 2
0 11124/99 5.3 39'0 11124/99 2625 135 20 -4010 0 0
11125/99 11125199 0 0 0 w 11126199 6.0 3860 32 11126199 2'80 139 " 2368 1 2
00 11127/99 11127/99 0 0 0
11128/99 59 3630 8 11128199 2m 12, '° 0 0
11129/99 11129199 0 20690 1 2
11/30/99 6.1 4370 ' 11/30'99 23'9 139 18 12750 0 0
AVG· 5.9 3727 11 AVG: 1392 167 « 9182 0 1
MAX: 7.0 4970 '° MAX: 26'9 218 78 20690 1 2 MIN 5.3 3040 ' MIN: 0 124 4 2170 0 0
DID NOT PROCESS SBR.
- -- - - - - - - -- -- - - - - -
--- - -- - - - - -- -- - - -- -
GROUNDWATER MONTHLY MONITORING: GROUNDWATER MONTHLY MONITORlN( INNER TIER EQUALIZATION TANK: ITEOT INNER TIER CARBON Fil TER EFFLUENT #81TEF PAGE NO. 2 PAGE NO. 7 NOVEMBER.1999 NOVEMBER.1999 DATE PH: COD: OTWATERADDED DATE: PH; COD: TOC: TSS: pH ppm '" pH ppm ppm ppm
11/01/99 7.7 3230 1111)1/99
11/02199 7.6 2980 11/02/99 11/03199 7.7 '290 350 11,{13/99 6.3 193 11 32 11""99 7.7 3630 11/04/99 11/05199 7.4 3520 11105199 11/06/99 7.2 3960 11/06/99 11/07/99 7.4 3220 1111'.17/99
11/08/99 7.7 3910 11"""'9 11/09199 7.4 3100 11"9199 8.2 172 10 11110/99 7.6 3270 11110/99 11111/99 7.6 3760 11/11/99 11112199 7.6 '"° 11112/99 11113/99 7.7 3360 375 11/13199 11114/99 7.9 3510 11114/99 11115199 7.6 3660 11/15199 11116199 7.6 4450 11116199
11117/99 7.4 ,oeo 11/17/99 6.2 \28
11118199 7.6 3570 375 11/18199
11/19/99 7.6 4330 11/19/99
0 11/20/99 7.5 4560 11/20l99
11/21/99 7.7 3580 11/21199
0 11122/99 7.6 4350 11/22199
11/23199 7.7 3140 11'23199 0 11/24199 7.5 3780 11124/99 6.2 113
0 11/25199 7.6 4080 11125199 11126199 7.6 4160 11/26199 w 11127/99 7.6 3970 11/27/99
(0 11/28199 7.6 3160 11,::26199
11129199 7.7 4080 11/29199 11130199 7.6 3080 563 11/30l99
AVG· 7.6 3746 416 AVG: 6.2 152 9 32 MAX: 7.9 4560 563 MA)t 6.3 193 \1 32 MIN: 7.2 2960 350 MIN· 6.2 113 7 32
GROUNDWATER MONTHLY MONITORING:
RAINFALL DATA
DATE INCHES/DAY
12/01/99 0.00
12/02/99 0.00
12/03/99 0.00
12/04/99 0.00
12/05/99 0.60
12/06/99 0.00
12/07/99 0.00
12/08/99 0.00
12/09/99 0.00
12/10/99 0.30
12/11/99 0.00
12/12/99 0.00
12/13/99 0.70
12/14/99 0.00
12/15/99 0.00
12/16/99 0.00
12/17/99 o.oo
12/18/99 0.00
12/19/99 0.10
12/20/99 0.00
12/21/99 0.80
12/22/99 0.00
12/23/99 o.oo
12/24/99 0.00
12/25/99 0.00
12/26/99 0.00
12/27/99 0.00
12/28/99 0.00
12/29/99 0.00
12/30/99 0.00
12/31/99 0.00
TOTAL 2.50
000040
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I INNER TIER
DAILY FLOW
I DEC.
1999 IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9
I 12/01/99 48 22 83 88 218 63 139 428 517
12/02/99 51 13 86 86 213 63 136 445 511
12/03/99 49 0 86 85 220 63 138 469 513 I 12/04/99 51 0 82 81 214 63 137 500 506
12/05/99 ·51 0 91 81 234 57 136 510 498
12/06/99 48 29 91 83 222 65 135 310 429
I 12/07/99 47 23 94 83 91 59 133 384 415
12/08/99 48 23 88 77 161 61 126 362 493
12/09/99 49 21 92 76 231 63 129 372 498
12/10/99 50 21 92 72 218 61 129 368 488
I 12/11/99 52 21 94 68 144 61 129 368 510
12/12/99 51 5 92 64 252 59 126 360 480
12/13/99 52 0 94 63 172 61 126 368 486
12/14/99 51 30 93 54 172 60 125 363 479
I 12/15/99 50 24 97 70 224 60 123 371 468
12/16/99 50 23 97 61 197 60 118 373 482
12/17/99 18 8 35 24 84 22 50 136 165
12/18/99 47 28 94 60 204 55 90 344 0 I 12/19/99 51 23 92 65 222 59 121 381 0
12/20/99 47 22 93 62 208 59 123 373 0
12/21/99 47 5 42 65 208 · 63 128 392 0
I 12/22/99 48 28 219 67 219 64 128 398 0
12/23/99 49 26 98 65 178 62 123 390 0
12/24/99 47 23 95 67 114 62 127 395 0
12/25/99 48 24 98 69 118 65 131 410 0
I 12/26/99 46 10 95 68 157 62 125 384 0
12/27/99 48 11 99 72 219 64 126 388 6
12/28/99 48 27 98 69 228 63 117 363 3
12/29/99 44 24 100 68 247 64 113 392 719
I 12/30/99 43 23 100 70 234 63 112 345 738
12/31/99 44 10 100 72 243 64 109 78 726
I AVG: 48 18 94 70 196 60 123 372 327
TOTAL: 1473 547 2910 2155 6066 1870 3808 11520 10130
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I 000041
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
ACTION
DATE WELL# PROBLEM DATE ACllON
12/6/99 #2 NO FLOW 12/6/99 RESET PUMP
12/6/99 #8 LOW FLOW 12/6/99 REPLACED BLADDER.METER& WATER LINE
12/29/99 #9 LOW FLOW 12/29/99 CLEANED PROBES & REPLACED METER
000042
MECHANIC
P.P.
P.P.
P.P.
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-------------------
0
0
0
0
~ w
OT-2R
OT-3
OT-4
OT-5
OT-6
OT-SA
OT-7
OT-8
Thermometer
Operational? ..
X
X
X
X
X
X
X
X
Monthly O&M Plan Checklist
HNA Holdings, Inc., Shelby, NC
Heat Lamp
Operational? ..
X
X
X
X
X
X
X
X
Other Operational Items/Comments
(-Temperature and HeRt Lamp checks October thru April only)
Form Completed by: __________ Tc..O=NY-'--=B'-'R'-'-Y'-'ANT'--'-'-----------
Date: 12/1/99 --------'-=-'-'---=-'"---------
I
DAILY REFERENCE SHEET: I
DATE: IT. EQ. PLT. DEC. DEC. WAS MIX MIX MIX NIT PHOS MIX F/M
DEC. INF. TNK. SEP. LIQ LIQ LIQ ADD ADD LIQ WAS 5/DAY I 1999 COD. COD. COD. COD. TSS. TSS MLSS NIT PHOS GALS LBS SET. GALS F/M AVG.
1 4530 2840 3940 126 36 4700 1696 97 18.8 1 2 50 40 0.21 I 2 5000 4020 5400 1916 104 20.2 0 0 50 40 0.00
3 3460 3490 3790 145 20 19890 1966 101 20.0 0 0 50 40 0,17
4 4500 3970 13300 1860 99 13.6 2 50 40 0.00
5 4800 4100 3850 141 36 7350 2020 106 22.8 0 0 50 40 0.17 0.11
6 4930 3500 16870 1492 97 14.2 1 2 50 40 0.00 0.07 I 7 4310 4770 3570 142 36 ~960 1728 111 20.8 0 0 50 40 0.18 0.10
8 4840 3780 2656 100 12.6 2 50 0 0.00 0.07
9 4400 4780 4020 136 32 5630 1956 114 20.2 2 100 40 0.18 0.11
10 4270 4170 2044 112 18.8 2 100 0 0.00 0.07 I 11 5220 4600 4780 153 32 14790 1972 126 27.5 0 100 40 0.22 0.12
12 7020 4780 1816 124 19.0 100 0 0.00 0.08
13 4710 4140 5400 161 48 19410 1888 135 18 .. 8 0 0 100 40 0.25 0.13
14 4720 4750 18470 1932 105 10.4 1 2 100 40 0.00 0.09
15 5110 4470 3820 142 16 20340 1452 141 19.6 0 2 100 40 0.23 0.14 I 16 4830 3810 1738 117 20.5 0 0 100 0 0.00 0.10
17 4980 4090 18410 2044 128 17.2 0 2 100 40 0.00 0.10
18 4920 4160 3790 124 56 18890 1892 137 22.4 0 0 100 40 0.18 0.08
19 7760 5220 2388 107 20.5 1 120 0 0.00 0.08 I 20 7500 5250 5390 152· 28 19700 2064 119 24.0 0 0 120 108 0.23 0.08
21 6690 5620 15690 2184 100 15.7 2 120 108 0.00 0.08
22 6950 5930 4760 172 60 10090 2120 117 18.4 0 0 120 108 0.20 0.12
23 6860 5680 15730 2044 120 18.0 120 108 0.00 0.09
24 10000 6300 5180 162 56 10930 1736 128 25.0 0 150 108 0.27 0,14 I 25 9300 5930 11320 1708 113 15.0 1 150 40 0.00 0.09
26 9460 6680 4640 164 140 11250 1728 136 25.3 0 0 150 40 0.24 0.14
27 8230 5670 10300 2096 237 20.0 0 0 150 40 0.00 0.10
28 6730 4980 160 44 10040 1980 168 16.0 0 0 150 54 0.22 0.15 I 29 10550 6180 9820 2060 118 17.5 1 150 54 0.00 0.09
30 3850 6560 4550 182 40 10770 1912 127 25.0 0 160 100 0.21 0.13
31 4660 4150 3980 164 44 9340 2228 125 18.3 0 0 150 54 0.16 0.12
AVG: 5971 4780 4144 143 43 12823 1946 121.6 18.6 104 48 0.11 I MAX: 10550 6680 5400 182 140 20340 2656 237.0 27.5 1 2 160 108 0.27
MIN: 3460 2840 0 0 0 4700 1452 97.0 0.0 0 0 50 0 0.00
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000044 I
-- - - --- - --- -- - - - - - -GROUNDWATER MONTHLY MONITORING: INNER TIER COMBINED INFLUENT #2 ITCI SBR MIXED LIQUOR: SBRML PAGE NO.1 PAGENO.4 DECEMBER.1999 OECEMBER.1999 SETT. SLUDGE 5/DAY DATE· FLOW. PH: coo TSS TOG: DATE: PH, NH3N: P04: oo, MLSS MLVSS: SOLIDS WASTED FIM. FIM GPO pH ppm ppm ppm pH ppm ppm ppm ppm ppm ma ,., -""' 12101,'99 1606 5.4 4530 27 133-0 12Al1/99 8.1 " 18.8 ◄.1 1698 50 " 0.21 12/02199 1504 5.4 5000 14 12/02199 8.0 104 20.2 3.8 1916 50 40 0.00 12/03/99 1623 S.4 3400 9 12/03199 8.0 101 20.0 S.S 1988 50 40 0.16 12/04199 1634 S.4 4500 t5 ,,_,, 8.0 99 13.6 ◄.7 "''" 50 40 0.00 12/05/99 1658 5.4 4800 17 12/05199 7.9 108 22.8 4.7 2020 50 40 0,17 0.11 12/06/99 1412 5.4 4930 t3 12/0M9 8.0 " 14.2 4.S 1492 50 40 0.00 0.07 12/07199 1329 5.3 4310 7 20SO 12itl7/99 7.9 111 20.8 5.7 1728 1500 50 "' 0.25 0.11 t2/0M9 1439 S.2 4840 5 1"""99 8.0 100 12.6 3.2 2658 50 0 000 0.08 12/09'99 1531 52 4400 4 12'0.,,, 7.9 114 20.2 ,.s 1958 too 40 0.18 012 12/10199 1499 S.2 4270 6 12110'99 8.0 112 18.8 5.7 2044 100 0 0.00 0.09 12/11/99 1447 5.0 S220 10 12111/99 8.0 128 27.5 4.0 1972 100 "' 0.22 0.13 12/12199 1489 5.0 7020 1t 12/12199 8.0 124 19.0 4.0 1816 100 0 0.00 0.08 12/13199 1422 5.4 4710 1t 12/13/99 8.t 135 18.8 5.2 1888 100 40 0.25 0.13 12/14199 1427 5.3 4720 9 12/1"'199 8.t 105 10.4 4.9 1932 1e2• 100 40 0.00 0.09 12/15199 1487 5.2 5110 8 1490 12/15199 8.t 1◄1 19.6 5.2 1452 100 40 0.23 0.1-1 12/16199 1481 5.3 4930 8 12/16199 8.t 117 20.5 •.8 1738 100 0 0.00 0.10 12/17199 542 5.2 4980 11 12117/99 8.t 128 17.2 5.◄ 2044 100 40 000 0.10 12/18/99 922 5.2 4920 t3 12118/99 8.t 137 22 .• 4.◄ 1892 100 40 0.18 0.08 12/19199 101• 5.2 7760 10 12119/99 8.1 107 20.5 3.9 2388 120 0 0.00 0.08 '.=:> 12120'99 987 52 7500 1t 12120'99 8.2 119 2•.o 5.1 2084 120 109 0.23 0.09 12121/99 950 5.2 8890 10 12121199 8.t 100 15.7 •• 2184 1672 120 108 000 0.08 :=> 12122/99 1171 5.2 8950 18 1880 12122199 9.2 117 16.4 4.5 2120 120 10B 0.20 0.12 0 12123/99 991 51 6880 48 12123'99 8.t 120 18.0 4.5 2044 120 109 0.00 0.09 12/2M99 930 5.1 10000 54 12124'99 8.1 128 25.0 3.9 1736 150 109 0.27 0.1• =:, 12/25199 963 50 9300 340 12125'99 8.0 113 15.0 4.8 1708 150 40 0.00 009 .i:,. 12/28199 947 5.1 9480 27 12128'99 8.t 136 25.3 4.9 1728 150 40 0,24 0.14 12/27199 1033 5.2 8230 30 12127199 8.t 237 20.0 4.1 2098 150 40 O.OC 0.10 U1 12/28/99 1016 5.3 6730 40 3210 12129/99 8.1 188 16.0 ◄.3 1980 1572 150 54 0.22 0.15 12129/99 1771 5.2 10550 t3 1"""" 8.t 118 17.5 4.• 2080 150 54 0.00 0.09 12,30m 1728 5.1 3850 282 12'30'99 8.2 127 25.0 4.1 1912 160 100 0.21 0.13 12131199 1448 5.2 4880 88 12131199 8.0 125 18.3 40 2228 150 " AVG: 1306 5.2 5971 37 1988 AVG: 8.t 122 19 5 1948 1592 104 48 0.11 0.10 MAX 1771 5.4 10550 340 3210 MAX: 8.2 237 28 • 2658 1872 160 108 0.27 0.15 MIN· 542 5.0 3460 4 1330 MIN: 7.9 97 to 3 1452 1500 50 0 0.00 0.07
GROUNOV/A TER MONTHLY MONITORING: GROUNDWATER MONTHLY MONITORING: AFTER PtA TE SEPARATOR BEFORE SBR: SBR! SBR EFFLUENT:(OECAND #4 SBRE PAGE NO. 3 PAGE NO, 5
DECEMBER.1999 OECEMBER.1999 WAS. NH3N PHOS. DATE: PH: COD: TSS: DATE: FLOW: COO: TSS: TSS ADDEO: ADDEO: pH ppm ppm GPO ppm ppm ppm gal lb>
12101'99 5.9 3940 20 12/01/99 2500 128 36 '700 1 2 12/02199 12')2199 0 5'00 0 0 12/03/99 6.2 3460 4 12/03199 2,,12 1'5 20 19890 0 0 12/04199 12/04199 0 13300 2 12/05199 54 3850 12/05199 2364 1'1 38 7350 0 0 12'Cel99 12""99 0 16870 12/07'99 5.2 4770 12/07/99 2"5 142 36 •960 0 0 12/08199 12/08199 0 2 12/09199 5.2 4020 12 12/09'99 2310 138 32 5630 2 12/1()(99 12/10/99 0 2 12111/99 6.9 478C 12/11/99 2409 153 32 14790 0 12112199 12/12199 0 1 1 12/1319!? S.9 5'00 48 12/13199 2'07 161 48 19410 0 0 12/W99 12/14/99 0 18470 2 12115199 5.8 3820 8 12/15199 2501 141 ,a 20340 0 2 12116199 12/16199 0 0 0 12/17/99 12/17/99 0 18410 0 2 12/18199 5.3 3790 28 12/18199 2513 124 56 1892 0 0 :i 12119199 12/19199 0 1 1 12/20/99 7.0 5390 80 12'20'99 2475 152 28 19700 0 0 :> 12121199 12121/99 0 """' 2 :> """" 5.3 4700 8 12'22Ml 2127 172 so 10090 0 0 1.2r.'.3/99 12'23/99 0 15730 ) 12/24/99 5.< 5180 16 1212-4199 2818 182 56 10930 0 12125199 12'25'99 0 11320 1 ~ 12125199 5.7 -0 8 12'2"'99 2103 104 140 11250 0 0 ) 12127199 12127/99 0 10300 0 0 12128199 5.5 4980 20 12'28199 2129 180 44 10040 0 0 12129199 12'29'99 0 9820 1 12130'99 5.8 4550 24 12/30'99 1971 182 40 10770 0 12/31/99 S.9 3980 20 12/31/99 2509 104 44 9340 0 0
AVG· 5.9 4457 19 AVG: 1231 152 " 12179 1 MAX 7.0 5400 80 MAX· 2818 182 140 20340 1 2 MIN: 5.2 3480 4 MIN: 0 124 ,a 1892 0 0
DID NOT PROCESS SBR.
---- - -- - - - -- - -- - -
-- - ---- - - - ---- -- ---
GROUNDWATER MONTHLY MONITORING: GROUNDWATER MONTHLY MONITORIN( INNER TIER EOUAUZATION TANK: ITEQT INNER TTER CARBON FILTER EFFLUENT #8 ITEF PAGE NO. 2 PAGE NO. 7 DECEMBER.1999 OECEMBER.1999 DATE· PH: COD: OT WATER ADDED DATE: PH: COD: TOC: TSS· pH ppm '" pH -ppm ppm
12/01199 7.7 2840 12/01/99 8.3 114 10 24 12/02/99 7.7 4020 ~2/02/99 1"1l3199 7.7 3490 12,1)3199 1"""99 7.7 3970 12,1)4199 12/05199 7.8 '100 1"1lS/99 12"""9 7.6 3500 1"""'99 12/07/99 7.5 mo 12JU7/99 8.1 129 11 1211:lB/99 7.5 3780 12/06199
12/09/99 7.4 4780 1=>199 12/10/99 7.6 4170 12/10199 12/11199 74 4600 12/11199 12/12/99 7A 4780 12/12199 12113199 7.6 4140 12/13199 12/14199 7.6 4750 12/14199 12/15199 7.4 4470 12/15199 18 12/16199 7.7 3810 12/16199 12117199 7.6 4750 12117/99 :=> 12118/99 7.4 '160 12/18199
12/19/99 7.6 5220 12119/99 => 12/20/99 7.6 5250 12120/99
0 12/21/99 7_-; 5620 12121/99 12122/99 7.3 5930 12122/99 8.2 137 18 => 12123199 7.7 5660 12123199
"" 12!24199 7.6 6300 "'°·' 1212""' 12125199 7.6 5930 12125/00 . ...:! 12125199 7.6 6680 450.0 12128/99 12127/99 7.6 5670 12/27199 121,e,w 7.4 413.0 12128199 8.0 164 19 12/29199 7.6 6180 12129/99 12/30'99 7.4 6560 12/30/99 12/31199 7.6 4150 450.0 12/31/99
AVG. 7.6 4802 403 AVG: 82 138 15 24 MAX 7.8 6680 ,so MAX: 8.3 164 19 24 MIN: 7.3 2840 300 MIN: 8.0 114 10 24
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I Attachment 2
I Analytical Data for the
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3rd and 4th Quarter 1999 Sampling Events
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I Kubal-Furr & Associates
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DATA ASSESSMENT CHECKLIST REPORT-LEVEL II
Client ID:
Project Number:
Moni taring Period:
Hoechst Celanese/Shelby
TFO26DB01
03/1999
Sample Delivery Group (SDG) Description:
Prepared By: Diane M. Davis
Date: 10/15/99
Quarterly monitoring well samples collected and analyzed by Davis & Floyd, Inc. of Greenwood,
SC. The samples collected were analyzed for volatiles and semivolatiles according to EPA
SW-846 methodology.
CONTENTS IEVEL COMMENTS
II
Sample Results v All data Class A except as noted
in the discussion section below.
Method Conformance Summary v O.K.
Chain(s) of Custody (COCs) v Various info incomplete. No
effect on data.
Master Tracking List v O.K.
Case Narrative
Sample Prep .
Standards Prep
Instrument Quality Control Data
Batch Quality Control Report v O.K. with the exceptions noted
in the discussion section below.
Surrogate Recovery Report
Trip/Field/Equipment Blank Report v O.K.
Field Notes/Logbook v Various info incomplete. No
effect on data.
CLP Forms
All Raw Data
Electronic Deliverables v O.K.
Discussion:
(1) The laboratory flagged the following results as estimated. Due to matrix interference, the
laboratory was unable to obtain a clear mass spectrum for the compounds specified. Based on
this, the following samples were flagged as indicated:
flag the 2-Butanone and Acetone results for sample ITCI.(lab ID#L99072310-03)
with a J.
flag the 2-Butanone, Acetone, and Vinyl Acetate results for sample V-23 (lab
ID#L99072310-15) with a J.
(2) The matrix spike/matrix spike duplicate for sample AA-54 (lab ID#L99072310-10) recovered
slightly below the laboratory established limits for 5 out of 10 spike compounds for 8260B.
The associated LCS met all recovery requirements. Based on this, sample AA-54 was flagged
as indicated:
-flag Benzene, Chlorobenzene, Toluene, and Trichloroethene with a J.
Class A = quantitative Class B = qualitative
J = estimated
Class C = unusable
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DAVIS
FL6YD
August 11, 1999
JERRY MCMURRAY
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
:L99072310
:60885.00
LABORATORY ANALYSIS REPORT
Login Number
Project Number
Description :GROUNDWATER SAMPLING & ANALYSIS
Dear Jerry Mcmurray:
We are pleased to provide the enclosed analytical results for the samples received by
Davis & Floyd, Inc. on July 23, 1999.
A formal Quality Assurance/Quality Control program is maintained by Davis & Floyd,
which is designed to meet or exceed the EPA or appropriate regulatory requirements.
All analytical analyses for this project met QA/QC criteria unless otherwise stated in the
footnotes. This report is to be reproduced only in full.
Feel free to contact our Client Services Representative at [phone] if further
explanation of the analysis is required. Unless other arrangements have been made, samples
will be disposed of or returned 14 days from the date of the report. We appreciate the
opportunity to provide services to your firm.
Sincerely, DAVIS;zz;
Jo n H. McCord, Jr.
aboratory Manager
000001 I Dav;s & Floyd, Inc. I PO Drawer 428 I Greenwood. SC 296411 I 816 E. Durst Avenue I Greenwood, SC 2%49 I [phone] I Fax (1\64) 229-7119
DA,YIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: HH-77
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1, 1, 2, 2-TETRACllLOROBTHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONB
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BR OMO FORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CflLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
NAPHTHALENE
STYRENE
TETRACHLOROETHENE
TOLUENE
GW/ChemW
NC Certification Number: 25
Project Number: 60885.00
Report Date Auguot 11, 1999
Page 1 of 2
Sample ID L99072310-01
Date Collected: 21-JUL-99 12 :00
Date Received 23-JUL-99
Result RDL Unite Analyst Date Time
18.0 1.0 degreeo c 07/21/99 1200
6.5 0.50 r:u 07/21/99 1200
92.0 1.0 umhon/cm 07/21/99 1200
715, 56 .01 feet MSL 07/21/99 1200
< 0 .010 X 0. 010 mg/1 PAP 07/27/99 0953
< 0. 010 X 0 .010 mg/1 PAP 07/27/99 09S3
< 0.010 X 0.010 mg/1 PAP 01/21/99 09S3
< 0. 010 X 0.010 mg/1 PAP 07/27/';J';J 0953
< 0. 010 X 0.010 mg/1 PAP 07/27/99 09S3
< 0. 010 X 0.010 mg/1 PAP 07/27/99 09S3
< 0.010 X 0 .010 mg/1 PAP 07/27/99 09S3
< 0.020 X 0.020 mg/1 PAP 07/27/99 09S3
< 0.020 X 0 . 020 mg/1 PAP 07/27/99 09S3
< 0.010 X 0.010 rng/1 PAP 07/27/99 09S3
< 0. 020 X 0 .020 mg/1 PAP 07/27/99 09S3
< 0. 010 X 0 .010 mg/1 PAP 07/27/99 09S3
< 0.010 X 0.010 rng/1 PAP 07/27/99 0953
< 0.010 X 0. 010 mg/1 PAP 07/27/99 09S3
< 0. 020 X 0.020 mg/1 PAP 07/27/99 09S3
< 0. 010 X 0.010 mg/1 PAP 07/27/99 09S3
< 0 .010 X 0. 010 mg/1 PAP 07/27/99 09S3
< 0.010 X 0. 010 mg/1 PAP 07/27/99 09S3
< 0 .020 X 0 .020 mg/1 PAP 07/27/99 09S3
< 0 .010 X 0.010 rng/1 PAP 07/27/99 0953
< 0 .020 X 0.020 mg/1 PAP 07/27/99 09S3
< 0.010 X 0 .010 mg/1 PAP 07/27/99 0953
0. 010 X 0 .010 mg/1 PAP 07/27/99 09S3
< 0 .010 X 0. 010 rng/1 PAP 07/27/99 0953
< 0. 010 X 0.010 mg/1 PAP 07/27/99 09S3
< 0 .010 X 0. 010 mg/1 PAP 07/27/99 09S3
< 0. 010 X 0.010 mg/1 PAP 07/27/99 0953
< 0. 010 X 0. 010 mg/1 PAP 07/27/99 0953
< 0 .010 X o. 010 mg/1 PAP 07/27/99 0953
0. 010 X 0.010 mg/1 PAP 07/27/99 09S3
000002
Davis & r-loyd, Inc. I PO Drawer 428 1 Greenwood, SC 29648 I 816 E. Durst Avenue j Greenwood, SC 29649 ! [phone] ! Fax [phone]
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DAYIS
FLtJYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: HH-77
Parameter
TRANS-1,2-DICHLOROETHBNE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHBNE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
NC Certification Number: 25
Project Number: 60B85.00
Report Date Auguot 11, 1999
Page 2 of 2
Sample ID L99072310-0l
Result Qual RDL Units Analyst Date Time
< 0 .010 X 0. 010 mg/1 PAP 07/27/99 0953
< 0. 010 X 0 .010 mg/1 PAP 07/27/99 0953
0.25 0.010 mg/1 PAP 07/27/99 0953
< 0 . 020 X 0.020 mg/1 PAP 07/27/99 0953
< 0 .020 X 0.020 mg/1 PAP 07 /27 /99 0953
< 0 .010 X 0. 010 mg/1 PAP 07/27/99 0953
000003
Davis & Floyd, Inc. 1 PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DA,YIS
FLtJYD LABORATORY ANALYSIS REPORT
client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: HH-48
Parameter
Field Data
EPA 170.l
TEMPERATURE
SW846 9040B
PH
SWB46 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SWB46 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICH!.OROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONB
2-HEXANONE
4-METHYL-2-PBNTANONB
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOPORM
BROMOMETHAN'E
CARBON DI.SULPIDF.
CARBON TBTRACHLORIDB
CHLOROBENZBNE
CHLOROETHANE
CHLOROFORM
CHLOROMBTHANE
CIS-1,2-DICHLOROETHENB
CIS-1, 3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
BTHYLBENZBNB
METHYLENE Cl!LORIDB
NAPHTHALENE
STYRBNB
TETRACHLOROETHENE
TOLUENE
GW/ChemW
NC Certification Number: 25
Result
19.0
s.,
63.0
715.44
' 0.0050
' 0.0050
' 0 . 0050
' 0.0050
' 0.0050
' 0 .0050
' 0 .0050
' 0.010
' 0.010
' 0.0050
' 0.010
' 0.0050
' 0.0050
' 0.0050
' 0.010
' 0.0050
' 0.0050
' 0 .0050
' 0. 010
' 0.0050
' 0.010
' 0.0050
' 0 .0050
' 0.0050
< 0.0050
' 0.0050
' 0.0050
' 0. 0050
' 0 .0050
' 0.0050
000004
Project Number: 60BB5.00
Report Date
Page 1 of 2
.Sample ID
Augu:Jt 11, 1::,99
L99072310-02
Date Collected: 21-JUL-99 12:06
Date Received 23-JUL-99
RDL Units Analyst Date Time
1.0 degrees C 07/21/99 1206
0.50 nu 07/21/99 1206
1.0 umho:J/cm 07/21/99 1206
.01 feet MSL 07/21/99 1206
0.0050 mg/1 PAP 07/27/99 1013
0 .0050 mg/1 PAP 07/27/99 1013
0.0050 mg/1 PAP 07/27/99 1013
0.0050 mg/1 PAP 07/27/99 1013
0 .0050 mg/1 PAP 07/27/99 1013
0.0050 mg/1 PAP 07/27/99 1013
0 .0050 mg/1 PAP 07/27/99 1013
0. 010 mg/1 PAP 07/27/99 1013
0 .010 mg/1 PAP 07/27/99 1013
0.0050 mg/1 PAP 07/27/99 1013
0.010 mg/1 PAP 07/27/99 1013
0.0050 mg/1 PAP 07/27/99 1013
0.0050 mg/1 PAP 07/27/99 1013
0.0050 mg/1 PAP 07/27/99 1013
0.010 mg/1 PAP 07/27/99 1013
0.0050 mg/1 PAP 07/27/99 1013
0.0050 mg/1 PAP 07/27/99 1013
0 .0050 mg/1 PAP 07/27/99 1013
0.010 mg/1 PAP 07/27/99 1013
0.0050 mg/1 PAP 07/27/99 1013
0.010 mg/1 PAP 07/27/99 1013
0.0050 mg/1 PAP 07/27/99 1013
0 . 0050 mg/1 PAP 07/27/99 1013
0 .0050 mg/1 PAP 07/27/99 1013
0.0050 mg/1 PAP 07/27/99 1013
0.0050 mg/1 PAP 07/27/99 1013
0.0050 mg/1 PAP 07/27/99 1013
0.0050 mg/1 PAP 07/27/99 1013
0 .0050 mg/1 PAP 07 /27 /99 1013
0.0050 mg/1 PAP 07/27/99 1013
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue 1 Greenwood, SC 29649 I [phone] I Fax {864) 229-7119
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DA,YIS
FLifYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: HH-48
Parameter
TRANS-1,2-0ICHLOROETHENE
TRANS-1,3-0ICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
<
<
<
<
<
NC Certification Number: 25
Project Number: 60885.00
Report Date
Page 2 of 2
Sample ID
August 11, 1999
Result Qual RDL Units Analyst Date
0.0050 0.0050 mg/1 PAP 07/27/99
0.0050 0.0050 mg/1 PAP 07/27/99
0. 084 0.0050 mg/1 PAP 07/27/99
0 .010 0. 010 mg/1 PAP 07 /27 /99
0. 010 0.010 mg/1 PAP 07/27/99
0.0050 0.0050 mg/1 PAP 07/27/99
000005·
Time
1013
1013
1013
1013
1013
1013
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-441 3 j Fax [phone]
DA,YIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Cont.act
TICONA,LLC
P.O. BOX 87
,'3HELBY, NC 28150
JERRY MCMURRAY
Client ID: ITCI
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
SW846 9050
M..itrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Ga.s Chromatography
SW846 8015
ETHYLENE GLYCOL
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1, 1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOPORM
BROMOMETHANE
CARBON DI.SULPIDE
CARBON TBTRACHLORIDB
CHLOROBENZENE
CHLOROETHANE
CHLOROPORM
CHLOROMETHANE
crn-1, 2-DICHr,OROETHENE
CIS-1, 3 •DI CHLOROPROPENE
DIBROMOCHLOROMETHANB
ETHYLBENZENE
METHYLENE CHLORIDE
GW/ChemW
NC Certification Number: 25
Project Number: 60885.00
Report Date Auguct 13' 1999
Page 1 of 2
Sample ID L99D72310-03
Date Collected: 21-JUL-99 12 ; so
Date Received 23-JUL-99
Reeult Qua.I RDL Units Analyst Date Time
NA 1.0 07 /21/99 1250
5.3 0.50 OU 07/21/99 1250
1850 1.0 umhoc/cm 07/21/99 1250
NA .01 feet MSL 07/21/99 1250
310 70.0 mg/1 JAW 08/02/99 1712
' 0.0050 0.0050 mg/1 PAP 07/27/99 1034
' 0.0050 0 .0050 mg/1 PAP 07/27/99 1034
' 0.0050 0.0050 mg/1 PAP 07/27/99 1034
' 0.0050 0.0050 mg/1 PAP 07/27/99 1034
' 0 . 0050 0.0050 mg/1 PAP 07/27/99 1034
' 0 .0050 0 .0050 mg/1 PAP 07/27/99 1034
' 0.0050 0.0050 mg/1 PAP 07/27/99 1034
0, 052 0. 010 mg/1 PAP 07/27/99 1034
' 0.010 0 .010 mg/1 PAP 07/27/99 1034
' 0.0050 0.0050 mg/1 PAP 07/27/99 1034
0. 095 0.010 mg/1 PAP 07/27/99 1034
0. 035 0 .0050 mg/1 PAP 07/27/99 1034
' 0.0050 0 .0050 mg/1 PAP 07/27/99 1034
' 0.0050 0. 0050 mg/1 PAP 07/27/99 1034
' 0.010 0.010 mg/1 PAP 07/27/99 1034
0.011 0.0050 mg/1 PAP 07/27/99 1034
' 0.0050 0.0050 mg/1 PAP 07/27/99 1034
0, 02 6 0.0050 mg/1 PAP 07/27/99 1034
' 0. 010 0.010 mg/1 PAP 07/27/99 1034
' 0.0050 0.0050 mg/1 PAP 07/27/99 1034
' 0. 010 0.010 mg/1 PAP 07/27/99 1034
' 0.0050 0.0050 mg/1 PAP 07/27/99 1034
0. 0050 0.0050 mg/1 PAP 07/27/99 1034
< 0.0050 0.0050 mg/1 PAP 07/27/99 1034
< 0.0050 0.0050 mg/1 PAP 07/27/99 1034
' 0 . 0050 0 . 0050 mg/1 PAP 07/27/99 1034
000006
Davis & Floyd, Inc. / PO Drawer 428 I Greenwood, SC 2964B I 816 E. Durst AVenue I Greenwood, SC 29649 I [phone] I Fax (B64} 229-7119
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FLtrYD LABORATORY ANALYSIS REPORT
NC Certification Number: 25
Client TICONA,LLC Project Number:
Contact
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITCI
Parameter
NAPHTHALENE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Wet. Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
Rea:ult
< 0 .0050
< 0.0050
< 0 .0050
< 0 .0050
< 0.0050
< 0 .0050
< 0 .0050
< 0. 010
< 0.010
< 0.0050
1530
Report Date
Page 2 of 2
Sample ID
Qu•l RDL
0 .0050
0 .0050
0.0050
0.0050
0 .0050
0.0050
0 .0050
0 .010
0 .010
0.0050
10.0
Sample Comments: • Entimation due to matrix interference. Unable to obtain a
clear mano npectrum for the compound.
The reoult for Ethylene Glycol should be conoidered ao
entimated. The analytical holding time wao exceeded. Thio
nample will be recollected for analyoio of Ethylene Glycol
and reported neparately.
000007
60885.00
Auguot 13, 1999
L99072310-03
Uni ta Analyst Date Time
mg/1 PAP 07/27/99 1034
mg/1 PAP 07 /27 /99 1034
mg/1 PAP 07/27/99 1034
mg/1 PAP 07/27/99 1034
mg/1 PAP 07/27/99 1034
mg/1 PAP 07/27/99 1034
mg/1 PAP 07 /27 /99 1034
mg/1 PAP 07/27/99 1034
mg/1 PAP 07/27/99 1034
mg/1 PAP 07/27/99 1034
mg/1 TRB 07/26/99 1132
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I Ul 6 [. Durst Avenue I Greenwood, SC 29(>49 I [phone] I Fax [phone]
DAVIS
FLt1YD LABORATORY ANALYSIS REPORT
client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: C-49
Parameter
Field Data
EPA 170.1
TEMPERATURE;
SW846 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND .WATER·ELEVATION
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CH LOR OM ETHANE
CIS-1, 2-DICHLOROETHENE
CIS-1, 3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
NAPHTHALENE
STYRENE
TETRACHLOROETHENE
TOLUENE
GW/ChemW
NC Certification Number: 25
Result
19.0
5.2
22.0
845.73
' 0.0050
' 0.0050
' 0 .0050
' 0 .0050
' 0.0050
' 0.0050
' 0.0050
' 0 .010
' 0.010
' 0.0050
' 0.010
' 0.0050
' 0 .0050
' 0.0050
' 0.010
' 0.0050
' 0.0050
' 0.0050
' 0.010
' 0.0050
' 0.010
' 0 .0050
' 0. 0050
' 0 .0050
' 0.0050
' 0.0050
' 0.0050
' 0 .0050
' 0 .0050
' 0.0050
000008
Project Number: 60885.00
Report Date
Page 1 of 2
Sample ID
Auguot 11, 1999
L99072310-04
Date Collected: 21-JUL-99 14:19
Date Received 23-JUL-99
RDL Units Analyst Date Time
1.0 degreeo C 07/21/99 1419
0.50 OU 07 /21/99 1419
1.0 umhoD/cm 07/21/99 1419
.01 feet MSL 07/21/99 1419
0 .0050 mg/1 PAP 07/27/99 1054
0 .0050 mg/1 PAP 07/27/99 1054
0 .0050 mg/1 PAP 07/27/99 1054
0 .0050 mg/1 PAP 07/27/99 1054
0 .0050 mg/1 PAP 07/27/99 1054
0 . 0050 mg/1 PAP 07/27/99 1054
0 . 0050 mg/1 PAP 07/27/99 1054
0. 010 mg/1 PAP 07/27/99 1054
0 .010 mg/1 PAP 07/27/99 1054
0.0050 mg/1 PAP 07/27/99 1054
0.010 mg/1 PAP 07/27/99 1054
0.0050 mg/1 PAP 07/27/99 1054
0.0050 mg/1 PAP 07/27/99 1054
0.0050 mg/1 PAP 07/27/99 1054
0.010 mg/1 PAP 07/27/99 1054
0.0050 mg/1 PAP 07/27/99 1054
0 .0050 mg/1 PAP 07/27/99 1054
0.0050 mg/1 PAP 07/27/99 1054
0.010 mg/I PAP 07/27/99 1054
0.0050 mg/1 PAP 07/27/99 1054
0.010 mg/1 PAP 07/27/99 1054
0.0050 mg/1 PAP 07/27/99 1054
0. 0050 mg/1 PAP 07/27/99 1054
0 .0050 mg/1 PAP 07/27/99 1054
0.0050 mg/1 PAP 07/27/99 1054
0 .0050 mg/1 PAP 07/27/99 10 54
0.0050 mg/1 PAP 07/27/99 1054
0.0050 mg/1 PAP 07/27/99 1054
0,0050 mg/1 PAP 07/27/99 1054
0 .0050 mg/1 PAP 07/27/99 1.054
Davis & f-=/oyd, Inc. I PO Drawer 428 I Greenwood, SC 29(,411 I 81 (, r:. Durst Avenue I Greenwood, SC 2%49 I (8(i4) 229-441 J I f'.ax (H64) 229-7119
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D~IS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
client ID: C-49
Parameter
TRANS-1, 2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACHTATE
VINYL CHLORIDE
XYLENE (TOTAL)
NC Certification Number: 25
Result
' 0.0050
' 0.0050
' 0. 0050
' 0.010
' 0.010
' 0.0050
000009
Project Number: 60885.00
Report Date
Page 2 of 2
Sample ID
Qual RDL
0.0050
0 .0050
0.0050
0 .010
0 .010
0.0050
Augu□t 11, 1999
L99072310-04
Units Analyst Date
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
Time
1054
1054
1054
1054
1054
1054
Davis & Floyd, Inc. I PO Drawer 428 l Greenwomi, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAcVIS
FLtfYD LABORATORY ANALYSIS REPORT
client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID; T-35
Parameter
Field Data
EPA 170.1
TEMPBRATURB
SW846 9040B
PH
SWB46 9050
Matrix
SPECIFIC CONDUCTIVI.TY
GROUND WATER ELEVATION
Volatile Organics
SW846 826GB
1,1,l-TRICHLOR08THANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROBTHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HBXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROM OM ETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMBTHANE
CTS-1,2-DICHLOROETHENE
CIS-1,3-DIC!ILOROPROPENB
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
NAPHTHALENE
STYRENE
TBTRACHLOROETHENE
TOLUENE
GW/ChemW
NC Certification Number: 25
Result
19.0
5,6
522
765. 71
' 0.0050
' 0.0050
' 0 .0050
' 0 .0050
' 0 .0050
' 0.0050
' 0.0050
' 0. 010
' 0.010
' 0.0050
' 0.010
' 0.0050
' 0.0050
' 0 .0050
' 0. 010
' 0 .0050
' 0.0050
' 0 .0050
' 0. 010
' 0.0050
' 0.010
' 0. 0050
' 0 .0050
' 0 .0050
0 . 0050
' 0 .0050
' 0 .0050
' 0.0050
' 0 .0050
' 0 .0050
000010
Project Number: 60885.00
Report Date
Page 1 of 2
Sample ID
Date Collected:
Date Received
Qual RDL
1.0
0.50
1. 0
.01
0.0050
0.0050
0 .0050
0 .0050
0 .0050
0 .0050
0 .0050
0.010
0.010
0.0050
0.010
0.0050
0 .0050
0 .0050
0.010
0.0050
0.0050
0 .0050
0.010
0.0050
0. 010
0.0050
0.0050
0.0050
0.0050
0.0050
0 .0050
0.0050
0.0050
0 .0050
Auguot 11, 1999
L99072310-05
21-JUL-99 15: 26
23-JUL-99
Units Analyst
degreeo C
OU
umhoo/cm
feet MSL
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
mg/1 PAP
Date Time
07/21/99 1526
07/21/99 1526
07/21/99 1526
07/21/99 1526
07/27/99 1114
07/27/99 1114
07 /27 /99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
07/27/99 1114
Davis & Floyd, Inc. I PO Drawer 428 ) Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 ] [phone] I Fax [phone]
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: T-35
Parameter
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
NC Certification Number: 25
Result
< 0.0050
< 0.0050
< 0 .0050
< 0. 010
< 0 .010
< 0.0050
000011
Project Number: 60885.00
Report Date
Page 2 of 2
Sample ID
RDL
0.0050
0.0050
0 .0050
0.010
0 .010
0.0050
Auguot 11, 1999
L99072310-05
Unite Analyst Date
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
Time
1114
1114
1114
1114
1114
1114
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLtfYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: EE-58
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
.9W846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SW846 8260B
1, 1, 1-TRICHLOROETHAN"E
1,1,2,2-TETRACl-!LOROETHANE
1,1,2-TRICHLOROETHANE
1, 1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1, 2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOF'ORM
BROMOMETHANE
CARBON DISULF'IDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROBTHANF.
CHLOROFORM
CHLOROMETHANE
ClS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
£THYLBENZENE
M£THYL8NE CHLORIDE
NAPHTHALENE
STYRENE
TETRACHLOROETHENE
TOLUENE
GW/ChemW
NC Certification Number: 25
Reeult
17. 0
6.7
91.0
758.34
' 0 .0050
' 0.0050
' 0.0050
' 0 , 0050
' 0. 0050
' 0.0050
' 0 , 0050
' 0 .010
' 0.010
' 0.0050
' 0.010
' 0.0050
' 0 .0050
' 0 .0050
' 0.010
' 0.0050
' 0 .0050
' 0 .0050
' 0.010
' 0.0050
0.010
' 0.0050
' 0.0050
' 0 .0050
' 0.0050
' 0.0050
' 0.0050
' 0 .0050
' 0 .0050
' 0 .0050
000012
Project Number: 60885. 00
Report Date
Page 1 of 2
Sample ID
Date Collected:
Date Received
Qual RDL
1.0
0.50
1. 0
.D1
0 .0050
0 .0050
0. 0050
0.0050
0.0050
0.0050
0.0050
0 .010
0 .010
0.0050
0.010
0 .0050
0.0050
0 .0050
0.010
0 .0050
0 . 0050
0 .0050
0.010
0.0050
0. 010
0.0050
0.0050
0.0050
0.0050
0 .0050
0.0050
0 .0050
0.0050
0 .0050
Auguat 11, 1999
L99072310-06
21-JUL-99 16 : 11
23-JUL-99
Unite Analyst Date Time
degreeo C 07/21/99 1611
SU 07/21/99 1611
umhoo/cm 07/21/99 1611
feet MSL 07/21/99 1611
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 113 5
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
mg/1 PAP 07/27/99 1135
Davis & Floyd, Inc. I PO Drawer 428 l Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I r:ax [phone]
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DAYIS
FLtwD LABORATORY ANALYSIS REPORT
client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: EE-SB
Parameter
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
NC Certification Number: 25
Result
' 0 .0050
' 0. 0050
' 0.0050
' 0.010
' 0 .010
' 0.0050
000013
Project Number: 60885.00
Report Date
Page 2 of 2
Sample IO
Qual RDL
0 .0050
0.0050
0.0050
0. 010
0 .010
0.0050
Auguot 11, 1999
L99072310-06
Units Analyst Date
mg/1 PAP 07/27/99
mg/1 PAP 07 /27 /99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
Time
1135
1135
1135
1135
1135
1135
Davis & Floyd, Inc. / PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29()49 I [phone] I Fzix [phone]
DA,YIS
FLtlYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
J8RRY MCMURRAY
Client ID: FF-34
Parameter
Field Data
EPA 170.1
TBMPERATURE
SW846 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BR OMO FORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZHNE
CHLOROBTHANE
CHLOROFORM
CHLOROMETHANH
CIS-1,2-DICHLOROETHHNE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETIIYLBENZENE
METHYLENE CHLORIDE
NAPHTHALENE
STYRENE
TETRACHLOROETHENE
TOLUENE
GW/ChemW
NC Certification Number: 25
Result
18.0
,.,
58.0
761.16
< 0 .0050
< 0 .0050
< 0.0050
< 0. 0050
< 0. 0050
< 0.0050
< 0.0050
< 0. 010
< 0. 010
< 0.0050
< 0.010
< 0.0050
< 0.0050
< 0.0050
< 0.010
< 0.0050
< 0 .0050
< 0.0050
< 0.010
< 0.0050
< 0.010
< 0 . 0050
< 0.0050
< 0 .0050
< 0.0050
< 0.0050
< 0 .0050
< 0.0050
< 0.0050
< 0.0050
000014
Project Number: 60885.00
Report Date
Page 1 of 2
Sample ID
Auguot 11, 1999
L9907231D-07
Date Collected: 21-JUL-99 17:16
Date Received 23-JUL-99
Qual RDL Units Analyst Date Time
l. 0 degrees C 07/21/99 1716
0.50 OU 07/21/99 1716
1 . 0 umhoo/cm 07/21/99 1716
.01 feet MSL 07/21/99 1716
0 .0050 mg/1 PAP 07/27/99 1155
0.0050 mg/1 PAP 07/27/99 1155
0 .0050 mg/1 PAP 07/27/99 1155
0.0050 mg/1 PAP 07/27/99 1155
0.0050 mg/1 PAP 07/27/99 1155
0.0050 mg/1 PAP 07/27/';.19 1155
0.0050 mg/1 PAP 07/27/99 1155
0.010 mg/1 PAP 07/27/99 1155
0.010 mg/1 PAP 07/27/99 1155
0.0050 mg/1 PAP 07/27/99 1155
0.010 mg/1 PAP 07/27/99 1155
0 . 0050 mg/1 PAP 07/27/99 1155
0.0050 mg/1 PAP 07/27/99 1155
0 .0050 mg/1 PAP 07/27/99 1155
0.010 mg/1 PAP 07/27/99 1155
0.0050 mg/1 PAP 07/27/99 1155
0 .0050 mg/1 PAP 07/27/99 1155
0.0050 mg/1 PAP 07/27/99 1155
0.010 mg/1 PAP 07/27/99 1155
0.0050 mg/1 PAP 07/27/99 1155
0.010 mg/1 PAP 07/27/99 1155
0.0050 mg/1 PAP 07/27/99 1155
0.0050 mg/1 PAP 07/27/99 1155
0.0050 mg/1 PAP 07/27/99 1155
0.0050 mg/1 PAP 07/27/99 1155
0.0050 mg/1 PAP 07/27/99 1155
0 . 0050 mg/1 PAP 07/27/99 1155
0 . 0050 mg/1 PAP 07/27/99 1155
0.0050 mg/1 PAP 07/27/99 1155
0 .0050 mg/1 PAP 07/27/99 1155
Davi!-i & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I BH> F.. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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DAYIS
FLi1YD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: FF-34
Parameter
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
NC Certification Number: 25
Reeult
' 0.0050
' 0 .0050
' 0.0050
' 0.010
' 0 .010
' 0.0050
000015
Project Number: 60885.00
Report Date
Page 2 of 2
Sample ID
Qual RDL
0.0050
0 .0050
0 .0050
0.010
0 .010
0.0050
Augunt 11, 1999
L99072310-07
Onita Analyst Date
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07 /27 /99
mg/1 PAP 07/27/99
Time
1155
1155
1155
1155
1155
1155
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29b49 I (B64) 229-4413 I Fax (B64) 229-7119
DAYIS
FLt1YD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: FF-62
Parameter
Field Data
EPA 170.l
TEMPERATURE
SW846 9040B
PH
SW846 9050
M.:1trix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-0ICHLOROETHANB
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1, 2-DICIILOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
NAPHTHALENE
.STYRENE
TETRACHLOROETHENE
TOLUENE
GW/ChemW
NC Certification Number: 25
Result
18.0
6.4
77 .0
760,71
< 0 .0050
< 0.0050
< D .0050
< 0. 0050
< 0 .0050
< 0.0050
< 0.0050
< 0.010
< 0 .010
< 0.0050
< 0.010
< 0 .0050
0. 0050
< 0 .0050
< 0.010
< 0.0050
< 0 .0050
< 0.0050
< 0.010
< 0.0050
< 0.010
< 0.0050
< 0.0050
< 0 .0050
< 0.0050
< 0 .0050
< 0 .0050
< 0.0050
< 0.0050
< 0.0050
000016
Project Number: 60885.00
Report Date
Page 1 of 2
Sample ID
Auguot 11, 1999
L99072310-0B
Date Collected: 21-JUL-99 17;25
Date Received 23-JUL-99
Qual RDL Unite Analyst Date Time
1.0 degreeo c 07/21/99 1725
a.so OU 07/21/99 1725
1.0 umho::i/cm 07/21/99 1725
. 01 feet MSL 07/21/99 1725
0 .0050 mg/1 PAP 07/27/99 1216
0 .0050 mg/1 PAP 07/27/99 1216
0.0050 mg/1 PAP 07/27/99 1216
0.0050 mg/1 PAP 07/27/99 1216
0 .0050 mg/1 PAP 07/27/99 1216
0.0050 mg/1 PAP 07/27/99 1216
0.0050 mg/1 PAP 07/27/99 1216
0.010 mg/1 PAP 07/27/99 1216
0.010 mg/1 PAP 07/27/99 1216
0.0050 mg/1 PAP 07/27/99 1216
0.010 mg/1 PAP 07/27/99 1216
0 .0050 mg/1 PAP 07/27/99 1216
0 .0050 mg/1 PAP 07/27/99 1216
0 .0050 mg/1 PAP 07/27/99 1216
0.010 mg/1 PAP 07/27/99 1216
0.0050 mg/1 PAP 07/27/99 1216
0 .0050 mg/1 PAP 07/27/99 1216
0.0050 mg/1 PAP 07/27/99 1216
0.010 mg/1 PAP 07/27/99 1216
0.0050 mg/1 PAP 07/27/99 1216
0.010 mg/1 PAP 07/27/99 1216
0 .0050 mg/1 PAP 07/27/99 1216
0.0050 mg/1 PAP 07/27/99 1216
0.0050 mg/1 PAP 07/27/99 1216
0.0050 mg/1 PAP 07/27/99 1216
0 .0050 mg/1 PAP 07/27/99 1216
0.0050 mg/1 PAP 07/27/99 1216
0.0050 mg/1 PAP 07/27/99 1216
0 .0050 mg/1 PAP 07/27/99 1216
0.0050 mg/1 PAP 07 /27 /99 1216
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2~l64B I II J Ci L Durs1 Avenue I Greenwood, SC 2<J64!J I (1164) 229-4413 I Fax [phone]
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DA,YIS
FLtlYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client IO: FF-62
Parameter
TRANS-1, 2 -DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
NC Certification Number: 25
Result
< 0.0050
< 0.0050
< 0.0050
< 0 .010
< 0.010
< 0.0050
000017
Project Number: 60885.00
Report Date
Page 2 of 2
Sample ID
RDL
0 .0050
0. 0050
0 .0050
0.010
0.010
0.0050
August 11, 1999
: L99072310-08
Units Analyst Date
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/';J9
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
Time
1216
1216
1216
1216
1216
1216
Davis & Floyd, lnc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I {864) 229-4413 I Fax (l\64) 229•7119
DAYIS
FLt1YD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX B7
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: GG-61
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1, 1-DICHLOROF.Tl!ANE
1,1-DICHLOROETHENE
1,2-DICHLOROETJ-IANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BR OMO FORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1, 2-lHCHI,OROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
NAPHTHALENE
STYRENE:
TETRACHLOROETHENE
TOLUENE
GW/ChemW
NC Certification Number: 25
Result
17.0
, ..
125
752.98
< 0.0050
< 0.0050
< 0.0050
< 0 .0050
< 0 .0050
< 0 . 0050
< 0.0050
< 0 .010
< 0 .010
< 0.0050
< 0.010
< 0 .0050
< 0.0050
< 0.0050
< 0.010
< 0.0050
< 0.0050
< 0.0050
< 0.010
< 0.0050
< 0.010
< 0.0050
< 0.0050
< 0.0050
< 0 . 0050
< 0.0050
< 0.0050
< 0 .0050
< 0.0050
< 0.0050
000018
Project Number: 60885.00
Report Date
Page 1 of 2
Sample ID
Auguct 11, 1999
L99072310-09
Date Collected: 22-JUL-99 10:17
Date Received 23-JUL-99
Qual RDL Units Analyst Date Time
1. 0 degree□ C 07/22/99 1017
0.50 DU 07/22/99 1017
1.0 umhos/cm 07/22/99 1017
. 01 feet MSL 07/21/99 1017
0 .0050 mg/1 PAP 07/27/99 1236
0.0050 mg/1 PAP 07/27/99 1236
0 .0050 mg/1 PAP 07/27/99 123 6
0 .0050 mg/1 PAP 07/27/99 1236
0.0050 mg/1 PAP 07/27/99 1236
o . 0050 mg/1 PAP 07/27/99 1236
0 .0050 mg/1 PAP 07/27/99 1236
0.010 mg/1 PAP 07 /27 /99 1236
0.010 mg/1 PAP 07/27/99 1236
0.0050 mg/1 PAP 07/27/99 1236
0.010 mg/1 PAP 07/27/99 1236
0 .0050 mg/1 PAP 07/27/99 1236
0.0050 mg/1 PAP 07/27/99 1236
0 .0050 mg/1 PAP 07/27/99 1236
0.010 mg/1 PAP 07/27/99 1236
0.0050 mg/1 PAP 07/27/99 1236
0.0050 mg/1 PAP 07/27/99 1236
0.0050 mg/1 PAP 07/27/99 1236
0.010 mg/1 PAP 07/27/99 1236
0.0050 mg/1 PAP 07/27/99 1236
0.010 mg/1 PAP 07/27/99 1236
0 .0050 mg/1 PAP 07/27/99 123 6
0 .0050 mg/1 PAP 07/27/99 1236
0.0050 mg/1 PAP 07/27/99 1236
0 . 0050 mg/1 PAP 07/27/99 1236
0.0050 mg/1 PAP 07/27/99 1236
0. 0050 mg/1 PAP 07/27/99 123 6
0. 0050 mg/1 PAP 07/27/99 1236
0.0050 mg/1 PAP 07/27/99 123 6
0.0050 mg/1 PAP 07/27/9:J 1236
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I B16 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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11
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DAYIS
FLtfYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: GG-61
Parameter
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-D!CHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYU:NE (TOTAL)
NC Certification Number: 25
Result
< 0. 0050
< 0. 0050
< 0.0050
< 0.010
< 0.010
< 0.0050
00001B
Project Number: 60885. 00
Report Date
Page 2 of 2
sample ID
Qual RDL
0.0050
0.0050
0.0050
0.010
0 .010
0.0050
Augunt 11, 1999
L99072310-09
Units Analyst Date
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
Time
1236
1236
1236
1236
1236
1236
Davis & r-!oyd, Inc. I PO Drawer 42B I Greenwood, SC 2964B I Bl 6 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLfrYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JE:RRY MCMURRAY
client ID: M-54
Parameter
Field Data
EPA 170 . .I
TEMPBRATURE_
SW846 9040B
PH
SW846 9050
Matrix
SPECIPIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile organica
SW84G 8260B
1, 1, 1·-TRICHLOROBTHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONB
BENZENB
BROMODICHLOROMETHANE
BROMOFORM
BROMOMBTHANB
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBHNZENE
CHLOROETHANE
CHLOROFORM
CHLOROME'_I'HANE
CtS-1,2-DICHLOROETHENE
CIS-1, 3 -DICHLOROPROPENE
DIBROMOCHLOROMETl!ANE
ETHYLBENZENE
METHYLENE CHLORIDE
NAPHTHALENE
STYRENE
TE'J'RACHLOROETl!ENE
TOLUENE
GW/Chemw
NC Certification Number: 25
Result
17.0
5.1
366
747,75
< 0. 0050
< 0.0050
< 0 .0050
< 0.0050
0.0050
< 0.0050
' 0.0050
< u .010
< 0.010
< 0.0050
< 0.010
< 0.0050
< 0 . 0050
< 0 .0050
< 0.010
< 0.0050
< 0.0050
< 0 . 0050
' 0.010
< 0.0050
< 0.010
< 0 .0050
< 0 .0050
< 0.0050
< 0.0050
0.032
< 0.0050
0 .0050
0 .0050
' 0 . 0050
000020
Project Number: 60885.00
Report Date
Page 1 of 2
Sample ID
August 11, 1999
L99072310-10
Date Collected: 22-JUL-99 10:58
Date Received 23-JUL-99
Qual RDL Units Analyst Date Time
1.0 degre'eo C 07/22/99 1058
a.so SU 07/22/99 1058
l. 0 umhoo/cm 07/22/99 1058
. 01 feet MSL 07/22/99 1058
0. 0050 mg/1 PAP 07/27/99 1257
0.0050 mg/1 PAP 07/27/99 1257
0.0050 mg/1 PAP 07/27/99 1257
0.0050 mg/1 PAP 07/27/99 1257
0.0050 mg/1 PAP 07/27/99 1257
0.0050 mg/1 PAP 07/27/99 1257
0.0050 mg/1 PAP 07/27/99 1257
0 .010 mg/1 PAP 07/27/99 1257
0 .010 mg/1 PAP 07/27/99 12 57
0.0050 mg/1 PAP 07/27/99 1257
0. 010 mg/1 PAP 07/27/99 1257
0.0050 mg/1 PAP 07/27/99 1257
0.0050 mg/1 PAP 07/27/99 1257
0 . 0050 mg/1 PAP 07/27/99 1257
0.010 mg/1 PAP 07/27/99 1257
0.0050 mg/1 PAP 07/27/99 1257
0.0050 mg/1 PAP 07/27/99 1257
0 . 0050 mg/1 PAP 07/27/99 1257
0.010 mg/1 PAP 07/27/99 1257
0.0050 mg/1 PAP 07/27/99 1257
0. 010 mg/1 PAP 07/27/99 1257
0.0050 mg/1 PAP 07/27/99 1257
0.0050 mg/1 PAP 07/27/99 1257
0 .0050 mg/1 PAP 07/27/99 1257
0 .0050 mg/1 PAP 07/27/99 1257
0 .0050 mg/1 PAP 07/27/99 1257
0.0050 mg/1 PAP 07/27/99 1257
0 .0050 mg/1 PAP 07/27/99 1257
0 .0050 mg/1 PAP 07/27/99 12 5 7
0.0050 mg/1 PAP 07/27/99 12 5 7
f?avis & Floyd, Inc. I 1'0 Drawer 42B I Greenwood, SC 2964H I 816 t. Durst Avenue I Greenwood, SC 2%49 I {H(J4) 229-4413 I Fax (f\()4} 229-7 ! 19
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D\YIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX B7
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: AA-54
NC Certification Number: 25
Project Number: 60885.00
Report Date
Page 2 of 2
Sample ID
Auguat 11, 1999
L99072310-10
Parameter Result Qual RDL Onits Analyst Date
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-0ICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
'
'
'
'
'
'
0.0050
0.0050
0.0050
0.010
0. 010
0.0050
Sillllple Comments: The MS/MSD for thio sample ohowed slightly low recoverieo
poaoibly due to matrix interference. The reoulto reported
should be considered as estimated.
000021
0.0050 mg/1 PAP 07/27/99
0.0050 mg/1 PAP 07/27/99
0.0050 mg/1 PAP 07/27/99
0. 010 mg/1 PAP D7/27/99
0.010 mg/1 PAP 07/27/99
0.0050 mg/1 PAP 07/27/99
Time
1257
1257
1257
1257
1257
1257
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I {864) 229-4413 I Fax [phone]
DAYIS
FLifYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JBRRY MCMURRAY
Client ID: P-58
Parameter
Field Data
EPA 170.1
TBMPERATURE
SW846 904GB
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1, 2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HBXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMSTHANE
CIS-1,2-DICHLOROETHENE
crn-1, J -DICHI,OROPROPHNE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
NAPHTHALENE
STYRENE
TETRACHLOROETHENE
TOLUENE
GW/ChemW
NC Certification Number: 25
Project Number: 60885.00
Report Date August 11, 1999
Page 1 of 2
Sample ID L99072310-ll
Date Collected: 22-JUL-99 12 :05
Date Received 23-JUL-99
Result Qual RDL Units Analyst Date Time
20.0 1.0 degreeo C 07/22/99 1205
,., 0.50 SU 07/22/99 1205
664 1.0 umho::;/cm 07/22/99 1205
763,96 .01 feet MSL 07 /22/99 1205
< 0 .0050 0 .0050 mg/1 PAP 07/27/99 1422
< 0.0050 0.0050 mg/1 PAP 07/27/99 1422
< 0.0050 0.0050 mg/1 PAP 07/27/99 1422
< 0 . 0050 0 .0050 mg/1 PAP 07/27/99 1422
< 0.0050 0 .0050 mg/1 PAP 07/27/99 1422
< 0.0050 0 .0050 mg/1 PAP 07/27/99 1422
< 0.0050 0.0050 mg/1 PAP 07/27/99 1422
< 0. 010 0 .010 mg/1 PAP 07/27/99 1422
< 0. 010 0.010 mg/1 PAP 07/27/99 1422
< 0.0050 0.0050 mg/1 PAP 07/27/99 1422
< 0. 010 0.01.0 mg/1 PAP 07/27/99 1422
< 0.0050 0 .0050 mg/1 PAP 07/27/99 1422
< 0 .0050 0 .0050 mg/1 PAP 07/27/99 1422
< 0 .0050 0 .0050 mg/1 PAP 07/27/99 1422
< 0.010 0.010 mg/1 PAP 07/27/99 1422
< 0.0050 0 .0050 mg/1 PAP 07/27/99 1422
< 0.0050 0 .0050 mg/1 PAP 07/27/99 1422
< 0 .0050 0.0050 mg/1 PAP 07/27/99 1422
< 0. 01.0 D. 010 mg/1 PAP 07/27/99 1422
< 0.0050 0.0050 mg/1 PAP 07/27/99 1422
< 0.010 0.010 mg/1 PAP 07/27/99 1422
< 0.0050 0. 0050 mg/1 PAP 07/27/99 1422
< 0.0050 0 .0050 mg/1 PAP 07/27/99 1422
< 0 .0050 0.0050 mg/1 PAP 07/27/99 1422
< 0.0050 0.0050 mg/1 PAP 07/27/99 1422
< 0 .0050 0.0050 mg/1 PAP 07/27/99 1422
0 .0050 0.0050 mg/1 PAP 07/27/99 1422
< 0.0050 0 .0050 mg/1 PAP 07/27/99 1422
< 0.0050 0 . 0050 mg/1 PAP 07/27/99 1422
< 0 .0050 0 .0050 mg/1 PAP 07/27/99 1422
000022
Davis & Floyd, Inc. I PO Drawer 428 l Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
client ID: P-58
Parameter
TRANS-1,2-D!CHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
'
'
'
'
'
'
NC Certification Number: 25
Result
0 .0050
0 .0050
0 .0050
0.010
0 .010
0.0050
Project Number: 60885.00
Report Date
Page 2 of 2
Sample ID
Qual RDL
0.0050
0.0050
0 .0050
0.010
0. 010
0.0050
Auguot. 11, 1999
L99072310-ll
Units Analyst Date
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
000023
Time
1422
1422
1422
1422
1422
1422
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 l 816 E. Durst Avenue I Greenwood, SC 29649 I {864) 229-4413 I Fax (864) 229•7119
DAYIS
FLt1YD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITEF
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Gas Chromatography
SW846 8015
ETHYLENE G!,YCOL
Volatile Organics
SW84G 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1, 1, 2-TRICHf,OROE'l'l!ANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHI,OROFORM
CHLOROMETHANE
CIS-1,2-~ICHLOROETHENE
CI.S-1, 3 -DlCHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CJ-ILORlDE
GW/ChemW
NC Certification Number: 25
Project Number: 60885.00
Report Date Auguot 13, 1999
Page 1 of 2
sample ID L99072310-12
Date Collected: 22-JUL-99 12 :30
Date Received 23-JUL-99
Result Qual RDL Onita Analyst Date Time
NA 1.0 degreeo c 07/22/99 1230
8.3 0.50 OU 07/22/99 1230
3430 1. 0 umho::i/cm 07/22/99 1230
NA .01 feet MSL 07/21/99 1230
18.0 7.0 mg/1 JAW 08/02/99 1226
0 .0050 0.0050 mg/1 PAP 07/27/99 1443
< 0 .0050 0.0050 mg/1 PAP 07/27/99 1443
< 0.0050 0.0050 mg/1 PAP 07/27/99 1443
< 0 . 0050 0.0050 mg/1 PAP 07/27/99 1443
< 0 .0050 0 .0050 mg/1 PAP 07/27/99 1443
< 0.0050 0.0050 mg/1 PAP 07/27/99 1443
< 0 . 0050 0.0050 mg/1 PAP 07/27/99 1443
< 0.010 0.010 mg/1 PAP 07/27/99 1443
< 0.010 0.010 mg/1 PAP 07/27/99 1443
< 0.0050 0.0050 mg/1 PAP 07/27/99 1443
< 0.010 0.010 mg/1 PAP 07/27/99 1443
< 0.0050 0 .0050 mg/1 PAP 07/27/99 1443
< 0 . 0050 0.0050 mg/1 PAP 07/27/99 1443
< 0.0050 0 .0050 mg/1 PAP 07/27/99 1443
< 0.010 0.010 mg/1 PAP 07/27/99 1443
< 0. 0050 0. 0050 mg/1 PAP 07/27/99 1443
< 0.0050 0.0050 mg/1 PAP 07/27/99 1443
< 0.0050 0.0050 mg/1 PAP 07/27/99 1443
< 0.010 0.010 mg/1 PAP 07/27/99 1443
0.0050 0.0050 mg/1 PAP 07/27/99 1443
< 0.010 0.010 mg/1 PAP 07/27/99 1443
< 0 . 0050 0.0050 mg/1 PAP 07/27/99 1443
< 0.0050 0 .0050 mg/1 PAP 07/27/99 1443
< 0 .0050 0.0050 mg/1 PAP 07/27/99 1443
< 0.0050 0.0050 mg/1 PAP 07/27/99 1443
0.033 0.0050 mg/1 PAP 07/27/99 1443
000024
Davis & Floyd, Inc. I PO Dr;'lwer 42H I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 \ [phone] I Fax [phone]
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DAcVIS
FLbYD LABORATORY ANALYSIS REPORT
NC Certification Number: 25
Client TICONA,LLC Project Number:
Contact
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client IO: ITEF
Parameter
NAPHTHALENE
STYRBNB
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROBTHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL}
Wet Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
'
'
'
'
'
'
'
'
'
'
Report
Page 2
Sample
Result Qual
0.0050
a .0050
0.0050
a. 0050
a. 0050
a. 0050
0.0050
0.010
0.010
0.0050
8.4
Sample CommentB: The re□ult for Ethylene Glycol nhould be considered as
entimated. The analytical holding time was exceeded. This
□ample will be recollected f.or analyni□ of. Ethylene Glycol
and reported neparately.
000025
Date
of 2
ID
RDL
0.0050
0.0050
0.0050
0.0050
a .0050
0.0050
0.0050
a .010
0.010
0.0050
1.0
60885.00
Augu::;t 13, 1999
L99072310-12
Units Analyst Date Tima
mg/1 PAP 07/27/99 1443
mg/1 PAP 07/27/99 1443
mg/1 PAP 07/27/99 1443
mg/1 PAP 07/27/99 1443
mg/1 PAP 07/27/99 1443
mg/1 PAP 07/27/99 1443
mg/1 PAP 07/27/99 1443
mg/1 PAP 07/27/99 1443
mg/1 PAP 07/27/99 1443
mg/1 PAP 07/27/99 1443
mg/1 TRB 07/26/99 1149
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2%4fl I 816 E. Durst Avenue I Greenwood, SC 29649 I (Hb4) 229-4413 I Fax (llfi4) 229-7119
DAYIS
FLt1YD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX B7
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITEF DUP.
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Gas Chromatography
SW846 8015
ETHYLENE GLYCOL
Volatile Organics
SW846 8260B
1, 1, 1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BlITANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1, 3 -DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
GW/Chemw
NC Certification Number: 25
NA
8.3
3430
NA
7.0
' 0. 0050
' 0 .0050
' 0.0050
' 0.0050
' 0 .0050
' 0.0050
' 0 .0050
0.010
' 0. 010
' 0.0050
' 0.010
' 0 .0050
' 0 .0050
' 0.0050
' 0.010
' 0.0050
0.0050
< 0 .0050
' 0.010
< 0.0050
< 0.010
' 0.0050
< 0.0050
0.0050
< 0.0050
0. 027
000026
Project Number: 60885.00
Report Date
Page 1 of 2
Sample ID
August 13, 1999
L99072310-1J
Date Collected: 22-JUL-99 12:30
Date Received 23-JUL-99
Qual RDL Units Analyst Date Time
1.0 degrees C 07/22/99 1230
0.50 SU 07/22/99 1230
1 . 0 umho::i/cm 07/22/99 1230
. 01 feet MSL 07/22/99 1230
7.0 mg/1 JAW 08/02/99 1249
o. 0050 mgn PAP 07/27/99 1503
0 . 0050 mg/1 PAP 07/27/99 1503
0.0050 mg/1 PAP 07/27/99 1503
0.0050 mg/1 PAP 07/27/99 1503
0 . 0050 mg/1 PAP 07/27/99 1503
0.0050 mg/1 PAP 07/27/99 1503
0 .0050 mg/1 PAP 07/27/99 1503
0.010 mg/1 PAP 07/27/99 1503
0.010 mg/1 PAP 07/27/99 1503
0.0050 mg/1 PAP 07/27/99 1503
0.010 mg/1 PAP 07 /27 /99 1503
0 .0050 ll"lg/1 PAP 07/27/99 1503
0.0050 mg/1 PAP 07/27/99 1503
0.0050 mg/1 PAP 07/27/99 1503
0.010 mg/1 PAP 07/27/99 1503
0.0050 mg/1 PAP 07/27/99 1503
0.0050 mg/1 PAP 07/27/99 1503
0. 0050 mg/1 PAP 07/27/99 1503
0.010 mg/1 PAP 07/27/99 1503
0.0050 mg/1 PAP 07/27/99 1503
0.010 mg/1 PAP 07/27/99 1503
0.0050 mg/1 PAP 07/27/99 1503
0.0050 mg/1 PAP 07/27/99 1503
0 .0050 mg/1 PAP 07/27/99 1503
0.0050 mg/1 PAP 07/27/99 1503
0.0050 mg/1 PAP 07/27/99 1503
Davis & Floyd, Inc. I PO Drawer 42H I Greenwood, SC 29(J48 I fll 6 E. Durst Avenue I Greenwood, SC 29649 I (a64) 229-4413 I Fax (Bh4) 22~J-7119
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DAYIS
FLtfYD LABORATORY ANALYSIS REPORT
NC Certification Number: 25
Client TICONA,LLC Project Number:
Contact
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITEF DUP.
Parameter
NAPHTHALENE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Wet Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
Report
Page 2
Sample
Result Quo1.l
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.010
' 0. 010
' 0.0050
'·'
Sample Comments: The reDult for Bthylene Glycol ohould be considered aD
eDtimated. The analytical holding time was exceeded. This
sample will be recollected for analysis of Ethylene Glycol
and reported separately.
000027
Date
of 2
ID
RDL
0.0050
0. 0050
0.0050
0.0050
0 .0050
0 .0050
0 .0050
0. 010
0.010
0.0050
1.0
60885.00
Augu:Jt 13, 1999
L99072310-13
Units Analyst Date Time
mg/1 PAP 07/27/99 1503
mg/1 PAP 07/27/99 1503
mg/1 PAP 07/27/99 1503
mg/1 PAP 07/27/99 1503
mg/1 PAP 07/27/99 1503
mg/1 PAP 07/27/99 1503
mg/1 PAP 07/27/99 1503
mg/1 PAP 07/27/99 1503
mg/1 PAP 07 /27 /99 1503
mg/1 PAP 07/27/99 1503
TRB 07/26/99 1330
Davis & Floyd, Inc. I PO Drawer 4211 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
o~i1s
FLOYD LABORATORY ANALYSIS REPORT
Client
Cont<1ct
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: K-28
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile OrganicG
SW846 8260B
1,1,1-TRICHLOROETI-IANE
1,1,2,2-TETRACHLOROBTHANE
1,1,2-TRICHLOROETHANE
1, 1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROBTHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
NAPHTHALENE
STYRENE
TETRACHLOROET!IENF.
TOLUENE
GW/ChemW
NC Certification Number: 25
19.0
6.5
265
792.01
< 0.0050
< 0.0050
< 0 .0050
< 0.0050
< 0 .0050
< 0.0050
< 0. 0050
< 0. 010
< 0. 010
< 0.0050
< 0.010
0.010
< 0 .0050
< 0.0050
< 0. 010
< 0.0050
< 0.0050
< 0 .0050
< 0.010
< 0.0050
< 0.010
0.0050
< 0.0050
< 0. 0050
< 0.0050
0,030
< 0. 0050
< 0.0050
< 0 .0050
< 0.0050
000028
Project Number, 60885.00
Report Date
Page 1 of 2
Sample ID
Augu:Jt 11, 1999
L99072310-14
Date Collected: 22-JUL-99 13:20
Date Received 23-JUL-99
Qual ROL Units Analyst Date Time
1.0 degree:J c 07/22/99 1320
0.50 SU 07/22/99 1320
1. 0 umhori/cm 07/22/99 1320
. 01 feet MSL 07 /22/99 1320
0 .0050 mg/1 PAP 07/27/99 1524
0.0050 mg/1 PAP 07/27/99 1524
0.0050 mg/1 PAP 07/27/9';J 1524
0. 0050 mg/1 PAP 07/27/99 1524
0.0050 mg/1 PAP 07/27/99 1524
0.0050 mg/1 PAP 07 /27 /';J';J 1524
0.0050 mg/1 PAP 07/27/99 1524
0.010 mg/1 PAP 07/27/99 1524
0.010 mg/1 PAP 07/27/99 1524
0.0050 mg/1 PAP 07/27/99 1524
0.010 mg/1 PAP 07/27/99 1524
0 . 0050 mg/1 PAP 07/27/99 1524
0 .0050 mg/1 PAP 07/27/99 1524
0 .0050 mg/1 PAP 07/27/99 1524
0.010 mg/1 PAP 07 /27 /99 1524
0.0050 mg/1 PAP 07/27/99 1524
0.0050 mg/1 PAP 07/27/99 1524
0.0050 mg/1 PAP 07/27/99 1524
0.010 mg/1 PAP 07/27/9';J 1524
0.0050 mg/1 PAP 07/27/99 1524
0. 010 mg/1 PAP 07/27/99 1524
0 .0050 mg/1 PAP 07/27/99 1524
0 .0050 mg/1 PAP 07/27/99 1524
0.0050 mg/1 PAP 07 /27 /99 1524
0.0050 mg/1 PAP 07/27/99 1524
0 .0050 mg/1 PAP 07/27/99 1524
0 .0050 mg/1 PAP 07/27/99 1524
.0050 mg/1 PAP 07/27/99 1524
0 .0050 mg/1 PAP 07/27/99 1524
0.0050 mg/1 PAP 07/27/99 1524
Davis & Floyd, Inc. PO Dr;iwer 42B I G1·eenwood, SC 2964H I B 16 E. Durst Avenue I Greenwood, SC 29649 \ (Hb4) 229-4413 I Fax (ll(,4) 229-7119
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DAYIS
FLtrYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: K-28
Pcrameter
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENB
VINYL ACETATE
VINYL CHLORIDE
XYLENB (TOTAL)
Wet Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
NC Certification Number: 25
Result
< 0 . 0050
< 0 .0050
< 0. 0050
< 0 .010
< 0. 010
< 0.0050
4.4
000029
Project Number: 60885.00
Report Date
Page 2 of 2
Sample IO
RDL
0 .0050
0 .0050
0 .0050
0. 010
0.010
0.0050
1.0
Auguat 11, 1999
L99072310-14
Units Analyst Date Time
mg/1 PAP 07/27/99 1524
mg/1 PAP 07/27/99 1524
mg/1 PAP 07/27/99 1524
mg/1 PAP 07/27/99 1524
mg/1 PAP 07/27/99 1524
mg/1 PAP 07/27/99 1524
mg/1 TRB 07/26/99 1349
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29(,49 I [phone] I Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Cont.act
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: V-23
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
SWB46 90S0
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile organics
SW846 8260B
1,1,l-TRICIILOROETHANE
1, 1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2 -PENTANONE
ACETONE
BENZENE
BROMOOICHLOROMETHANE
BROMOFORM
BROMOMBTHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
ClS-1,2-DIC!ILOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZBNE
METHYLENE CHLORIDE
NAPHTHALENE
STYRENB
TETRACHLOROETHENE
TOLUENE
GW/ChemW
NC Certification Number: 25
Project Number: 60885.00
Report Date Augu:::t 11, 1999
Page 1 of 2
Sample ID L99072310-15
Date Collected: 22-JUL-99 13 : 57
Date Received 23-JUL-99
Result RDL Units Analyst Date Time
19.0 1.0 degreeo C 07/22/99 1357
5.1 a.so OU 07/22/99 1357
6610 1 . 0 umhon/cm 07/22/99 1357
796.49 feet MSL 07/22/99 1357
' 0 .015 X 0 .015 mg/1 PAP 07/27/99 1849
' 0. 015 X 0 .015 mg/1 PAP 07/27/99 1849
' 0. 015 X 0. 015 mg/1 PAP 07/27/99 1849
0. 015 X 0 .015 mg/1 PAP 07/27/99 1849
' 0 .015 X 0 .015 mg/1 PAP 07/27/99 1849
' 0. 015 X 0 .015 mg/1 PAP 07/27/99 1849
' 0. 015 X 0 .015 mg/1 PAP 07/27/99 1849
0.27 0.030 mg/1 PAP 07/27/99 1849
' 0. 030 X 0. 030 mg/1 PAP 07/27/99 1849
' 0.015 X 0 .015 mg/1 PAP 07/27/99 1849
0.27 0 .030 mg/1 PAP 07/27/99 184 9
0.018 0. 015 mg/1 PAP 07/27/99 1849
' 0. 015 X 0.015 mg/1 PAP 07/27/99 1849
' 0 .015 X 0 .015 mg/1 PAP 07/27/99 1849
' 0. 030 X 0.030 mg/1 PAP 07/27/99 1849
' 0. 015 0.015 mg/1 PAP 07/27/99 1849
' 0 .015 X 0. 015 mg/1 PAP 07/27/99 184 9
' 0 .015 X 0.015 mg/1 PAP 07/27/99 1849
' 0.030 X 0. 030 mg/1 PAP 07/27/99 1849
' 0.015 X 0. 015 mg/1 PAP 07/27/99 1849
' 0. 030 X 0. 03 0 mg/1 PAP 07/27/99 1849
0 .015 X 0.015 mg/1 PAP 07/27/99 1849
' 0 .015 X 0 .015 mg/1 PAP 07/27/99 1849
' 0 .015 X 0 .015 mg/1 PAP 07/27/99 1849
' 0 .015 X 0 .015 mg/1 PAP 07/27/99 1849
' 0.015 X 0.015 mg/1 PAP 07/27/99 184 9
' 0.015 X 0.015 mg/1 PAP 07/27/99 1849
0 .015 X 0.015 mg/1 PAP 07/27/99 1849
' 0 .015 X 0.015 mg/1 PAP 07/27/99 1849
' 0. 015 X 0 .015 mg/1 PAP 07/27/99 1849
0000:30
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2964B I 816 E. Durst Avenue I Greenwood, SC 29649 I {864) 229-4413 I Fax [phone]
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DA,YIS
FLOYD LABORATORY ANALYSIS REPORT
NC Certification Number: 25
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: V-23
Parameter
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Wet Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
Result
< 0.015
< 0. 015
< 0 .015
0.54
' 0. 030
< 0. 015
9620
Project Number:
Report. Date
Page 2 of 2
Sample ID
Qual RDL
X 0.015
X 0.015
X 0. 015
0.030
X 0 .030
X 0 .015
10.0
Sample Comments: • E~timation due to matrix interference. Unable to obtain a
clear maoo opectrum for the compound.
()110131
60885.00
AuguEJt 11, 1999
L99072310-15
Unite Analyst Date Time
mg/1 PAP 07/27/99 1849
mg/1 PAP 07/27/99 1849
mg/1 PAP 07/27/99 1849
mg/1 PAP 07/27/99 1849
mg/1 PAP 07/27/99 1849
mg/1 PAP 07/27/99 1849
mg/1 TRB 07/26/99 1410
Davis & Floyd, Inc. I PO Dr;iwer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
o~i1s
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX B7
,SHELBY, NC 28150
JERRY MCMURRAY
Client ID: CC-33
Parameter
Field Data
EPA 170.1
TEMPERATURE
SWB46 9040B
PH
SWB46 9050
M,1trix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Volatile Organics
SW846 8260B
1,1,l-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1, 1-DICHLOROETHENE
1,2-DICHLOROETIIANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOF'ORM
BROMOMETHANE
CARBON DI.SULF'IDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHAflE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHAflE
ETHYLBENZENE
METHYLENE CHLORIDE
NAPHTHALENE
STYRENE
TETRACHLOROETHENE
TOLUENE
GW/ChemW
NC Certification Number: 25
Result
18.0
6 .s
366
788.57
< 0.0050
< 0 .0050
< 0.0050
< 0.0050
< 0 .0050
< 0 .0050
< 0.0050
< 0.010
< 0.010
< 0.0050
< 0.010
< 0.0050
< 0 .0050
< 0.0050
< 0.010
< 0.0050
< 0 . 0050
< 0.0050
0. 010
< 0.0050
< 0.010
< 0.0050
< 0.0050
< 0.0050
< 0 .0050
0.011
< 0.0050
< 0.0050
< 0.0050
< 0 .0050
000032
Project Number: 60885.00
Report Date
Page 1 of 2
August 11, 1999
Sample ID L99072310-16
Date Collected: 22-JUL-99 14:27
Date Received 23-JUL-99
Qual RDL Units Analyst Date Time
1.0 degrees C 07/22/99 1427
0.50 OU 07/22/99 1427
1. 0 umhon/cm 07/22/99 1427
. 01 feet MSL 07/22/99 1427
0.0050 mg/1 PAP 07/27/99 1605
0 .0050 mg/1 PAP 07/27/99 1605
0 .0050 mg/1 PAP 07/27/99 1605
0.0050 mg/1 PAP 07/27/99 1605
0 .0050 mg/1 PAP 07/27/99 1605
0 .0050 mg/1 PAP 07/27/99 1605
0.0050 mg/1 PAP 07/27/99 1605
0.010 mg/1 PAP 07 /27 /99 1605
0 .010 mg/1 PAP 07/27/99 1605
0.0050 mg/1 PAP 07/27/99 1605
0. 010 mg/1 PAP 07/27/99 1605
0.0050 mg/1 PAP 07/27/99 1605
0 .0050 mg/1 PAP 07/27/99 1605
0 .0050 mg/1 PAP 07/27/99 1605
0.010 mg/1 PAP 07 /27 /99 1605
0.0050 mg/1 PAP 07/27/99 1605
0 .0050 mg/1 PAP 07/27/99 1605
0 .0050 mg/1 PAP 07/27/99 1605
0.010 mg/1 PAP 07/27/99 1605
0.0050 mg/1 PAP 07/27/99 1605
0.010 mg/1 PAP 07/27/99 1605
0 .0050 mg/1 PAP 07/27/99 1605
0.0050 mg/1 PAP 07/27/99 1605
0.0050 mg/1 PAP 07/27/99 1605
o. 0050 mg/1 PAP 07/27/99 1605
0 .0050 mg/1 PAP 07/27/99 1605
0.0050 mg/1 PAP 07/27/99 1605
0. 0050 mg/1 PAP 07 /27 /99 1605
0 .0050 mg/1 PAP 07/27/99 1605
0 .0050 mg/1 PAP 07/27/99 1605
Davis & r:Joyd, Inc. / PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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D~IS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. SOX 87
.SHELBY, NC 2B150
JERRY MCMURRAY
Client ID: CC-33
Parameter
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE:
XYLENE {TOTAL)
NC Certification Number: 25
Result
' 0.0050
' 0 .0050
' 0.0050
' 0.010
' 0 .010
' 0.0050
000033
Project Number: 60885.00
Report: Date
Page 2 of 2
Sample ID
Qual RDL
0 . 0050
0 .0050
0.0050
0 .010
0.010
0.0050
Augu:::it 11, 1999
L99072310-16
Units Analyst Date
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
Time
1605
1605
1605
1605
1605
1605
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax (8&4) 229-7119
DAIIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: PEW-4
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
Matrix
SWB46 9050
SPECIFIC,CONDUCTIVITY
GROUND WATER ELEVATION
Semivolatile Organics
GW/ChemW
SW846 8270C
1,2,4-TRICHLOROBENZENE
1,2-0ICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DICHLOROPHENOL
2,4-DIMETHYLPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-METHYL-4,6-DlNITROPHENOL
2-METHYLNAPHTHALENE
2-MBTHYLPHENOL
2-NITROANILINB
2-NITROPHENOL
3,3'-DICHLOROBBNZIDINE
3-NITROANILINE
4-BROMOPHENYL PHENYL ETHER
4-CHLORO-3 -METHYLPHENOL
4-CHLOROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-METHYLPHENOL
4-NITROANILINE
4-NITROPHENOL
ACENAPHTHENB
ACENAPHTHYLENE
ANTHRACENE
NC Certification Number: 25
Project Number: 60885.00
Report Date Auguot 11, 1999
Page 1 of 4
Sample ID L99072310-17
Date Collected: 22-JUL-99 15; 15
Date Received 23-JUL-99
Result Qual RDL Units Analyst Date Time
22.0 1.0 degrees C 07/22/99 1515
'.1 0.50 OU 07/22/99 1515
112 1.0 umhoo/cm 07/22/99 1515
813.41 . 01 feet MSL 07/22/99 1515
< 0 .010 0. 010 mg/1 JRN/DSD 08/03/99 1222
< 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1222
< 0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1222
< 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1222
< 0.010 0.010 mg/1 JRN/DSD 08/03/99 1222
< 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1222
< 0. 010 0. 010 mg/1 JRN/DSD 08/03/99 1222
< 0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1222
< 0. 025 0.025 mg/1 JRN/DSD 08/03/99 1222
' 0.010 0. 010 mg/1 JRN/DSD 08/03/99 1222
< 0. 010 0. 010 mg/1 JRN/DSD 08/03/99 1222
' 0.010 0. 010 mg/1 JRN/DSD 08/03/99 1222
< 0 . 010 0 . 010 mg/1 JRN/DSD 08/03/99 1222
< 0. 025 0.025 mg/1 JRN/DSD 08/03/99 1222
< 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1222
< 0 .010 0. 010 mg/1 JRN/DSD 08/03/99 1222
< 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1222
< 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1222
< 0. 010 0. 010 mg/i JRN/DSO 08/03/99 1222
< 0. 010 0. 010 mg/1 JRN/DSD 08/03/99 1222
< 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1222
< 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1222
< 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1222
< 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1222
< 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1222
< 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1222
' 0. 025 0 .025 mg/1 JRN/DSD 08/03/99 1222
< 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1222
< 0.010 0.010 m9/l ,1RN/□so 08/03/99 1222
0. 010 0.010 mg/1 JRN/DSD 08/03/99 1222
000034
Davis & rloyd, Inc. I l'O Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax (B(i4) 229-7119
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DAYIS
FLtfYD LABORATORY ANALYSIS REPORT
NC Certification Number: 25
client TICONA,LLC Project Number: 60885.00
P.O. BOX 87
SHELBY, NC 28150 Report Date Auguot 11, 1999
Contact JERRY MCMURRAY Page 2 of 4
Client ID: PEW-4 Sample ID L99072310-17
Parameter Result Qu11.l RDL Units Analyst Date Time
BBNZO(A)ANTHRACENE ' 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1222
BBNZO(A)PYRENE ' 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1222
BENZO(B)FLUORANTHENE ' 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1222
BENZO(G,H,I)PERYLENE ' 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1222
BENZO(K)FLUORANTHENB ' 0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1222
BENZOIC ACID ' 0.050 0.050 mg/1 JRN/DSD 08/03/99 1222
BENZYL ALCOHOL ' 0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1222
BIS(2-CHLOROETHOXY)METHANE ' 0. 010 0. 010 mg/1 JRN/DSD 08/03/99 1222
BIS(2-CHLOROETHYL)ETHER ' 0.010 0. 010 mg/1 JRN/DSD 08/03/99 1222
BIS(2-CHLOROISOPROPYL)ETHER ' 0 .010 0.010 mg/1 JRN/DSD OB/03/99 1222
BIS(2-ETHYLHEXYL)PHTHALATE ' 0.010 0. 010 mg/1 JRN/DSD OB/03/99 1222
BUTYL BENZYL PHTHALATE ' 0.010 0. 010 mg/1 JRN/DSD OB/OJ/99 1222
CHRYSENE ' 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1222
DI-N-BUTYL PHTHALATB ' 0. 010 0 .010 mg/1 JRN/DSD 0B/03/99 1222
DI-N-OCTYL PHTHALATE ' 0. 010 0.010 mg/1 JRN/DSD 0B/03/99 1222
DIBENZ(A,H)ANTHRACENE ' 0. 010 0.010 mg/1 JRN/DSD OB/03/99 1222
DIBENZOFURAN ' 0 .010 0 .010 mg/1 JRN/DSD OB/03/99 1222
DIETHYL PHTHALATE ' 0. 010 0 .010 mg/1 JRN/DSD 0B/03/99 1222
DIMETHYL PHTHALATE ' 0.010 0.010 mg/1 JRN/DSD OB/03/99 1222
FLUORANTHENE ' 0 .010 0.010 mg/1 JRN/DSD OB/03/99 1222
FLUORENE ' 0 .010 0.010 mg/1 JRN/DSD OB/03/99 1222
HEXACHLOROBENZENB ' 0. 010 0.010 mg/1 JRN/DSD OB/03/99 1222
HEXACHLOROBIITADIENE ' 0.010 0.010 mg/1 JRN/DSD 0B/03/99 1222
HEXACHLOROCYCLOPENTADIENE ' 0.010 0 .010 mg/1 JRN/DSD OB/03/99 1222
HEXACHLOROETHANE ' 0. 010 0. 010 rng/1 JRN/DSD OB/03/99 1222
INDENO(l,2,3-CD)PYRENE ' 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1222
ISOPHORONE ' 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1222
N-NITROSODI-N-PROPYLAMINE ' 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1222
N-NITROSODIPHENYLAMINE ' 0 .010 0 .010 mg/1 JRN/DSD 0B/03/99 1222
NAPHTHALENE ' 0 .010 0 .010 mg/1 JRN/DSD OB/03/99 1222
NITROBENZENE ' 0 . 010 0 . 010 mg/1 JRN/DSD 0B/03/99 1222
PENTACHLOROPHENOL ' 0.025 0.025 mg/1 JRN/DSD 08/03/99 1222
PHENANTHRENE ' 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1222
PHENOL ' 0.010 0.010 mg/1 JRN/DSD 08/03/99 1222
PYRENE ' 0.010 0.010 mg/1 JRN/DSD 08/03/99 1222
SW846 8270C DOWTHERM
1,1'-BIPHENYL 0.011 0 .010 mg/1 DSD/JRN 0B/06/99 1011
BIPHENYL ETHER 0.033 0.010 mg/1 DSD/JRN OB/06/99 1011
000035
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 I:. Durst Avenue \ Greenwood, SC 29649 I [phone] I Fax [phone]
DA,YIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: PEW-4
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROBTHANE
1, 1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1, 1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETON8
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULF'IDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHl,OROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETl!YLBENZENE
METHYLENE CHLORIDE
NAPHTHALENE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1, 3 -DICHl,OROPROPENE
TRICHLOROSTHENB
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
NC Certification Number: 25
Result
0 .0050
' 0. 0050
' 0.0050
' 0.0050
' 0. 0050
' 0.0050
' 0.0050
' 0.010
' 0.010
0.0050
' 0.010
' 0.0050
' 0.0050
' 0.0050
' 0. 010
' 0.0050
' 0.0050
' 0.0050
' 0.010
' 0.0050
' 0.010
0, 015
' 0 .0050
' 0 .0050
' 0 .0050
0.031
' 0 .0050
' 0. 0050
' 0.0050
' 0 .0050
' o. 0050
' 0 .0050
0.050
' 0.010
' 0 .010
' 0.0050
000036
Project Number: 60885.00
Report Date
Page 3 of 4
Sample ID
Qual RDL
0.0050
0.0050
0.0050
0 . 0050
0 .0050
0 . 0 050
0.0050
0.010
0.010
0.0050
0. OlO
0.0050
. 0050
0.0050
0.010
0 .0050
0.0050
0 .0050
0. 010
0.0050
0.010
0 . 0050
0 .0050
0 .0050
0 .0050
0 .0050
0.0050
0.0050
0.0050
0.0050
0. 0050
0 .0050
0. 0050
0.010
0 .010
0.0050
Augu~t 11, 19~9
L99072310-17
Units Analyst Date
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
rng/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg /1 PAP 07/27/99
mg/1 PAP 07/27/99
rng/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07 /27 /<J<J
mg/1 PAP 07/27/99
Time
1626
1626
1626
1626
1626
1626
1626
1626
1626
1626
1626
1626
1626
1626
1626
1626
1626
162 6
1626
162 6
1626
1626
1626
1626
1626
1626
162 6
1626
1626
162 6
162 6
1626
1626
1.62 6
1626
1626
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 81 h E. Durst Avenue I Greenwood, SC 2%49 I [phone] I Fax [phone] I
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DAjIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JBRRY MCMURRAY
Client ID: PEW-4
Prep Procedure
Analytical Prep Procedures:
BNA SBMIVOLATILES
OOWTHERM
Method
SW846 35008
SW846 35008
NC Certification Number: 25
Project Number: 60885.00
Report Date Augu:Jt. 11, 1999
Page 4 of 4
Sample ID
Analyst Prep Oat•
JMT 07/27/99 0830
JMT 07 /27 /99 0830
000037
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DA,YIS
FLt1YD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: PEW-4 DUP.
Parameter
Field Data
J,.'PA 170.1
TEMPBRATURE
SW846 9040B
PH
SW846 9050
Matrix
SPECIPIC CONDUCTIVITY
GROUND WATER ELEVATION
Somivolatile Organics
SW846 8270C
1,2,4-TRICHLOROBENZENE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2, 4-DICHLOROPHENOL
2, 4-DIMETHYLPHENO!,
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-METHYL-4,6-DINTTROPHENOL
2-METHYLNAPHTHALENE
2-METHYLPHENOL
2-NITROANILINE
2-NITROPHENOL
3, 3' -DICJ-ILOROBBNZIDINE
3-NITROANILINE
4-BROMOPHENYL PHENYL ETHER
4-CHLOR0-3-METHYLPHENOL
4 -CHLOROANI LINE
GW/ChemW
4 -CHLOROPHENYL PHENYL: ETHER
4-METHYLPHENOL
4-NITROANILINE
4-NITROPHENOL
ACENAPHTHENE
ACENAPHTHYLENE
ANTJ-IRACBNE
NC Certification Number: 25
Result
22.0
6.1
112
813.41
< 0.010
< 0.010
0.010
< 0.010
< 0.010
< 0 .010
< 0.010
< 0.010
< 0.025
< 0.010
< 0 .010
< 0 .010
< 0. 010
< 0 .025
' 0. 010
' 0.010
< 0.010
< 0.010
< o. 010
< 0. 010
< 0 . 010
< 0.010
< 0 .010
< 0. 010
< 0.010
' 0.010
< 0.025
' 0.010
' 0.010
' 0. 010
000038
Project Number: 60885.00
Report Date
Page 1 of 4
Sample ID
Auguot 11, 1999
L99072310-18
Date Collected: 22-JUL-99 15:15
Date Received 23-JUL-99
Qual RDL Units Analyst Date Time
1.0 degreeo C 07/22/99 1515
0.50 07/22/99 1515
l.O umhoo/cm 07/22/99 1515
. 01 feet MSL 07/22/99 1515
0.010 mg/1 JRN/DSD 08/03/99 1300
0.010 mg/1 JRN/DSD 08/03/99 1300
o. 010 mg/1 JRN/DSD 08/03/99 1300
0. 010 mg/1 JRN/DSD 08/03/99 1300
0.010 mg/1 JRN/DSD 08/03/99 1300
0 .010 mg/1 JRN/DSD 08/03/99 1300
0 .010 mg/1 JRN/DSD 08/03/99 1300
0. 010 rng/1 JRN/DSD 08/03/99 1300
0. 025 mg/1 JRN/DSD 08/03/99 1300
0.010 mg/1 JRN/DSD 08/03/99 1300
0 .010 mg/1 JRN/DGD 08/03/99 1300
0 .010 mg/1 JRN/DSD 08/03/99 1300
0.010 mg/1 JRN/DSD 08/03/99 1300
0 . 025 mg/1 JRN/0S0 08/03/99 1300
0.010 mg/1 JRN/DSD 08/03/99 1300
0.010 mg~l JRN/DSD 08/03/99 1300
0.010 mg/1 JRN/DSD 08/03/99 1300
0.010 mg/1 JRN/DSD 08/03/99 1300
0.010 mg/1 JRN/DSD 08/03/99 1300
0.010 mg/1 JRN/DSD 08/03/99 1300
0 . 010 mg/1 JRN/DSD 08/03/99 1300
0.010 mg/1 JRN/DSD 08/03/99 1300
0.010 mg/1 JRN/DSD 08/03/99 1300
0. 010 mg/1 JRN/DSD 08/03/99 1300
0 .010 mg/1 JRN/DSD 08/03/99 1300
0 .010 mg/1 JRN/DSD 08/03/99 1300
0. 025 mg/1 JRN/DSD 08/03/99 1300
0. 010 mg/1 JRN/DSD 08/03/99 1300
0.010 mg/1 JRN/D.'JD 08/03/99 1300
0.010 mg/1 JRN/DSD 08/03/99 1300
0ovis & floycl, Inc. j PO Drowcr 428 I Greenwood, SC 2%48 j 8l6 E. Durst Avenue I Greenwood, SC 2%49 I [phone] I Fax [phone]
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DAVIS
FLfJYD LABORATORY ANALYSIS REPORT
NC Certification Number: 25
Client TICONA,LLC Project Number: 60885.00
P.O. BOX 67
SHELBY, NC 28150 Report Date Augunt 11, 1999
Contact JERRY MCMURRAY Page 2 of 4
Client ID: PEW-4 DUP. Sample ID L99072310-18
Parameter Result Qual RDL Onita Analyst Data Time
BENZO(A)ANTHRACENE ' 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1300
BBNZO (A) PYRENE ' 0.010 0.010 mg/1 JRN/DSD 08/03/99 1300
BENZO(B)FLUORANTHENE ' 0 .010 0 .010 mg/1 JRN/DSD 00/03/99 1300
BENZO(G,H,I)PERYLENE ' 0.010 0.010 mg/1 JRN/DSD 08/03/99 1300
BENZO{K)FLUORANTHENE ' 0 .010 0. 010 mg/1 JRN/DSD 08/03/99 1300
BENZOIC ACID ' 0 .050 0.050 mg/1 JRN/0S0 DB/03/99 1300
BENZYL ALCOHOL ' 0.010 0.010 mg/1 JRN/DSD 08/03/99 1300
BIS(2-CHLOROETHOXY)METHANE ' 0.010 0.010 mg/1 JRN/DSD 08/03/99 1300
BIS(2-CHLOROETHYL)ETHER ' 0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1300
BIS(2-CHLOROISOPROPYL)ETHER ' 0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1300
8IS(2-ETHYLHEXYL)PHTHALATE ' 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1300
BUTYL BENZYL PHTHALATE 0.010 0.010 mg/1 JRN/DSD 08/03/99 1300
CHRYSENE ' 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1300
DI-N-BUTYL PHTHALATE ' 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1300
DI-N-OCTYL PHTHALATE ' 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1300
DIBENZ(A,H)ANTHRACENE ' 0. 010 0. 010 mg/1 JRN/DSD 08/03/99 1300
DIBENZOFURAN ' 0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1300
DIETHYL PHTHALATE ' 0.010 0.010 mg/1 JRN/DSD 08/03/99 1300
DIMETHYL PHTHALATE ' 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1300
FLUORANTHENE ' 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1300
FLUORENE ' 0 .010 0. 010 mg/1 JRN/DSD 08/03/99 1300
HEXACHLOROBENZENE ' 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1300
HEXACHLOROBUTADIENE ' 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1300
HEXACHLOROCYCLOPENTADIENE ' 0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1300
HEXACHLOROETHANE ' 0.010 0. 010 mg/1 JRN/DSD 08/03/99 1300
INDENO (1, 2, 3-CD) PYRENE ' 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1300
ISOPHORONE ' 0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1300
N-NITROSODI-N-PROPYLAMINE ' 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1300
N-NITROSODIPHENYLAMINE ' 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1300
NAPHTHALENE ' 0.010 0. 010 mg/1 JRN/DSD 08/03/99 1300
NITROBENZENE ' 0.010 0.010 mg/1 JRN/DSD 08/03/99 1300
PENTACHLOROPHENOL ' 0.025 0.025 mg/1 JRN/DSD 08/03/99 1300
PHENANTHRENE ' 0 .010 0. 010 mg/1 JRN/DSD 08/03/99 1300
PHENOL ' 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1300
PYRENE ' 0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1300
SW846 8270C DOWTHERM
1, l' -BI PHENYL ' 0.010 0.010 mg/1 DSD/JRN 08/06/99 1048
BIPHENYL ETHER 0.026 0. 010 mg/1 DSD/JRN 08/06/99 1048
00O03~}
Davis & r:loyd, Inc. I PO Drawer 428 / Greenwood, SC 29648 I 816 E. Durst Avenue ! Greenwood, SC 29649 I [phone] I 1:ax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JBRRY MCMURRAY
Client ID: PEW-4 DUP.
Parameter
Volatile Organics
SW84G 8260B
1,1,1-TRICHLOROETHANE
1, 1, 2, 2-TETRACHLOROETHANE
1,1,2-TRICHLOROETf!ANE
1,1-DICHLOROETHANE
1, 1 -DICl!LOROETH!sNE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONB
2-HEXANONE
4-METHYL-2-PENTANONE
ACBTONE
BENZENE:
BROMODICHLOROMETHANE
BR OMO FORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBBNZENE
CIILOROETHANE
CHLOROFORM
CHLOROMHTHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMET!-IANE
ETHYLBENZENE
METHYLENE CHLORIDE
NAPHTHALENE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
NC Certification Number: 25
Result
' 0.0050
' 0.0050
' 0 .0050
' 0.0050
' 0.0050
' 0 .0050
' 0 . 0050
' 0.010
' 0. 010
' 0.0050
' 0.010
' 0. 0050
' 0.0050
' 0. 0050
0. 010
' 0.0050
' 0 .0050
' 0.0050
' 0.010
' 0.0050
' 0.010
0.015
' 0 .0050
' 0 .0050
' 0.0050
0.036
' 0.0050
' 0 . 0050
' 0.0050
' 0 . 0050
' 0 .0050
' 0.0050
0.049
' 0.010
' 0 .010
' 0.0050
000041)
Project Number: 60885.00
Report Date
Page 3 of 4
Augunt 11, 1999
Sample ID L99072310-18
Qual RDL Units Analyst Date
0.0050 mg/1 PAP 07/27/99
0. 0050 mg/1 PAP 07/27/99
0.0050 mg/1 PAP 07/27/99
0 .0050 mg/1 PAP 07/27/99
0.0050 mg/1 PAP 07/27/99
0.0050 mg/1 PAP 07/27/99
0 . 0050 mg/1 PAP 07/27/99
0 .010 mg/1 PAP 07/27/99
0.010 mg/1 PAP 07/27/99
0.0050 mg/1 PAP 07/27/99
0.010 mg/1 PAP 07/27/99
0. 0050 mg/1 PAP 07/27/99
0 . 0050 mg/1 PAP 07/27/99
0.0050 mg/1 PAP 07/27/99
0.010 mg/1 PAP 07/27/99
0. 0050 mg/1 PAP 07/27/99
0.0050 mg/1 PAP 07/27/99
0. 0050 mg/1 PAP 07/27/99
0. 010 mg/1 PAP 07/27/99
0.0050 mg/1 PAP 07/27/99
0. 010 mg/1 PAP 07/27/99
0 .0050 mg/1 PAP 07/27/99
0 .0050 mg/1 PAP 07/27/99
0. 0050 mg/1 PAP 07/27/99
o. 0050 mg/1 PAP 07/27/99
0 .0050 mg/1 PAP 07/27/99
0 .0050 mg/1 PAP 07/27/99
0 .0050 mg/1 PAP 07/27/99
0.0050 mg/1 PAP 07/27/99
0 .0050 mg/1 PAP 07/27/99
0 .0050 mg/1 PAP 07/27/99
0.0050 mg/1 PAP 07/27/99
0.0050 mg/1 PAP 07/27/99
0.010 mg/1 PAP 07/27/99
0.010 mg/1 PAP 07/27/99
0.0050 mg/1 PAP 07/27/99
Time
1647
1647
1647
1647
1647
1647
1647
1647
1647
1647
164 7
1647
1647
1647
1647
1647
1647
1647
1647
1647
1647
1647
1.647
1647
1647
1.647
1647
1647
1647
1647
164 7
1647
1647
1647
1647
1647
Davis & Floyd, Inc. I PO Drawer 428 l Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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DAYIS
FLi1YD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: PEW-4 DOP.
Prep Procedure
Analytical Prep Procedure•:
BNA SEMIVOLATILES
DOWTHERM
Method
SW846 3500B
SW846 35008
NC Certification Number: 25
Project Number: 608B5.00
Report Date Auguot 11, 1999
Page 4 of 4
Sample ID L99072310-1B
Analyat Prep Date
JMT 07/27/99 0830
JMT 07/27/99 0830
Davis & Floyd, Inc. I PO Drawer 420 I Greenwood, SC 29648 I 816 F.. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLiJYD LABORATORY ANALYSIS REPORT
Client TICONA,LLC
Contact
P.O. BOX 87
SHELBY, NC 28150
·JERRY MCMURRAY
Client ID: PEW-3
Parameter
Field Data
EPA 17D.l
TEM PBRATURE
SW846 9040B
PH
SWB46 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Semivolatile Organics
SWB46 8270C
1, 2, 4-TRICHLOROBE:NZENE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHBNOL
2,4,6-TRICHLOROPHENOL
2, 4-0ICHLOROPHENOL
2,4-DIMETHYLPHENOL
2, 4-DINITROPl!ENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-METHYL-4,6-DINITROPHBNOL
2-METHYLNAPHTHALENE
2-METHYLPHENOI,
2-NITROANILTNE
2-NITROPHENOL
3,3'-DICHLOROBENZIDINB
3-NITROANILINE
4-Bl<OMOPHENYL PHENYI, ETHER
4-CHLOR0-3-METHYLPHENOL
GW/ChcmW
4 -CHLOROANI LINE
4-CHLOROPHENYL PHENYL ETHER
4-METHYLPHENOL
4-NITROANILINB
4-NITROPHBNOL
ACENAPHTHENE
ACENAPllTHYLENE
ANTHRACENE
<
<
<
<
<
<
<
<
<
<
<
<
<
<
'
'
<
<
<
<
<
<
<
<
<
<
' <
<
NC Certification Number: 25
Project Number: 60885.00
Report Date Augu~t 11, 1999
Page 1 of 4
sample ID L99072310-19
Date Collected: 22-JUL-99 16: 24
Date Received 23-JUL-99
Result Qual RDL Units Analyst Date Time
22.0 1. 0 degreeo c 07/22/99 1624
6,9 0.50 OU 07/22/99 1624
54.0 1. 0 umhoo/cm 07/22/99 1624
811. 74 . 01 feet MSL 07/22/99 1624
0 .010 0.010 mg/1 JRN/DSD 08/03/99 1339
0. 010 0.010 mg/1 JRN/DSD 08/03/99 1339
0 .010 0. 010 mg/1 JRN/DSD 08/03/99 1339
0.010 0.010 mg/1 JRN/DSD 08/03/99 1339
0 . 010 0 . 010 mg/1 JRN/DSD 08/03/99 1339
0.010 0.010 mg/1 JRN/DSD 08/03/99 1339
0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1339
0.010 0.010 mg/1 JRN/DSD 08/03/99 1339
0. 025 0. 02 5 mg/1 JRN/DSD 08/03/99 1339
0.010 0 .010 mg/1 JRN/DSD 08/03/99 1339
0.010 0.010 mg/1 JRN/DSD 08/03/99 1339
0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1339
0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1339
0.025 0. 025 mg/1 JRN/DSD 08/03/99 1339
0.010 0.010 mg/1 JRN/DSD 08/03/99 1339
0.010 0.010 mg/1 JRN/DSD 08/03/99 1339
0 . 010 0 . 010 mg/1 JRN/DSD 08/03/99 1339
0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1339
0.010 0. 010 mg/1 JRN/DSD 08/03/99 1339
0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1339
.010 0 .010 mg/1 JRN/DSD 08/03/99 1339
0 .010 0 .010 mg/1 JRN/DSD 08/03/99 133 9
0.010 0. 010 mg/1 JRN/DSD 08/03/99 1339
0 .010 0.010 mg/1 JRN/DSD 08/03/99 1339
0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1339
0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1339
0 .025 0 . 025 mg/1 JRN/DSD 08/03/99 1339
0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1339
0.010 0. 010 mg/1 JRN/0S0 08/03/99 1339
0 .010 0.010 mg/1 JRN/DSD 08/03/99 1339
000042
Davis & Floyd, Inc. I 1'0 Drdwer 42/l I Greenwood, SC 29fi4H I 8Hi E. Durst Avenue I Greenwood, SC 29(i4'.) I (a64) 22~J-4413 I Fax (H64) 229-7119
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DAYIS
FLt1YD LABORATORY ANALYSIS REPORT
NC Certification Number: 25
Client TICONA,LLC Project Number: 60885.00
P.O. BOX 87
SHELBY, NC 28150 Report Date Augunt 11, 1999
Contact JERRY MCMURRAY Page 2 of 4
Client ID: PEW-3 sample ID L99072310-19
Parameter Result Qual RDL Uni ta Analyst Date Time
BENZO(A)ANTHRACENE < 0 . 010 0 . 010 mg/1 JRN/DSD 08/03/99 1339
BENZO{A) PYRENE < 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1339
BENZO(B)FLUORANTHENE < 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1339
BENZO(G,H,I)PERYLENE < 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1339
BENZO(K)FLUORANTHENE < 0.010 0. 010 mg/1 JRN/DSD 08/03/99 1339
BBNZOIC ACID < 0.050 0 .050 mg/1 JRN/DSD 08/03/99 1339
BENZYL ALCOHOL < 0.010 0. 010 mg/1 JRN/DSD OB/03/99 1339
BIS(2-CHLOROETHOXY)METHANE < 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1339
BIS(2-CHLOROETHYL)ETHER < 0.010 0.010 mg/1 JRN/DSD 08/03/99 1339
BIS(2-CHLOROISOPROPYL)ETHER < 0.010 0. 010 mg/1 JRN/DSD 08/03/99 1339
BIS(2-ETHYLHEXYL)PHTHALATE < 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1339
BlITYL BENZYL PHTHALATB < 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1339
CHRYSENE < 0 . 010 0 . 010 mg/1 JRN/DSD 08/03/99 1339
DI-N-BUTYL l'HTHALATE < 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1339
DI-N-OCTYL PHTHALATB < 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1339
DIBBNZ(A,H)ANTHRACENB < 0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1339
DIBBNZOF'URAN < 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1339
DIETHYL PHTHALATE < 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1339
DIMETHYL PHTHALATE < 0.010 0. 010 mg/1 JRN/DSD 08/03/99 1339
F'LUORANTHEN8 < 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1339
F'LUORENE < 0.010 0.010 mg/1 JRN/DSD 08/03/99 1339
HEXACHLOROBENZENE < 0.010 0.010 mg/1 JRN/DSD 08/03/99 1339
HEXACHLOROBUTADIENE < 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1339
HBXACHLOROCYCLOPENTADIBNE < 0.010 0.010 mg/1 JRN/DSD 08/03/99 1339
HEXACHLOROF.THANE < 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1339
INDENO(l,2,3-CO}PYRENE < 0.010 0. 010 mg/1 JRN/DSD 08/03/99 1339
ISOPHORONE < 0.010 0. 010 mg/1 JRN/OSO 08/03/99 1339
N-NITROSOOI-N-PROPYLAMINB < 0.010 0.010 mg/1 JRN/DSD 08/03/99 1339
N-NITROSODIPHF.NYLAMINE < 0.010 0.010 mg/1 JRN/0S0 08/03/99 1339
NAPHTHALENE < 0.010 0. 010 mg/1 JRN/DSD 08/03/99 1339
NITROBENZENB < 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1339
PENTACHLOROPHENOL < 0.025 0 .025 mg/1 JRN/DSD 08/03/99 1339
PHENANTHRENB < 0 .010 0. 010 mg/1 JRN/DSD 08/03/99 1339
PHENOL < 0.010 0.010 mg/1 JRN/0S0 08/03/99 1339
PYRENE < 0.010 0.010 mg/1 JRN/DSD 08/03/99 1339
SW846 B270C DOWTHERM
1, l' -BI PHENYL < 0.010 0.010 mg/1 DSD/JRN 08/06/99 1124
BIPHENYL ETHER < 0. 010 0.010 mg/1 DSD/JRN 08/06/99 1124
000043
Davis & Floyd, Inc. I PO Drawer 428 \ Greenwood, SC 29&48 I 816 E. Durst Avenue ! Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLtrYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 2B150
JERRY MCMURRAY
Client ID: PEW-3
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1, 1, 2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1, 2-DICHLORO['ROPANB
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DI.SULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1, 3-DICHLOROPROPENE
OIBROMOCHLOROMETHANE
8THYL88NZ8NE
METHYLENE CHLORIDE
NAPHTHALENE
.'JTYR8NE
TETRACHLOROETHENE
TOLUENE
TRAN.'J-1, 2 -DICHLOROETHEN8
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
NC Certification Number: 25
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Result
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.010
0.010
0.0050
0. 010
0 .0050
0.0050
0.0050
0.010
0. 0050
0 .0050
0 .0050
0.010
0.0050
0.010
0.0050
0 .0050
0.0050
0.0050
0.020
0.0050
0 .0050
0 . 0050
0.0050
0.0050
0 .0050
0.0050
0. 010
.010
0.0050
000044
Project Number: 608B5. 00
Report Date
Page 3 of 4
Sample ID
RDL
0.0050
0. 0050
0.0050
0 .0050
0 .0050
0.0050
0 .0050
0.010
0. 010
0.0050
0.010
0 .0050
0.0050
0 .0050
0.010
0 . 0050
0 .0050
0 .0050
0.010
0.0050
0.010
0.0050
0 .0050
0 .0050
0.0050
0. 0050
0 .0050
0.0050
0.0050
0 .0050
0 .0050
0.0050
0 .0050
0.010
0.010
0.0050
Augunt 11, 1999
L99072310-19
Units Analyst Date
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP D7/27/99
mg/_1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
, mg/1 PAP 07/27/99
mg/1 PAP 07/27/99
Time
1707
1707
1707
1707
1707
1707
1707
1707
1707
1707
1707
1707
1707
1707
1"707
1707
1707
1707
1707
1707
1707
1707
1707
1707
1707
1707
1707
1707
1707
1707
1707
1707
1707
1707
1707
1707
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29(148 j 816 E. Durst Avenue I Greenwood, SC 29649 I {864) 229-4413 I Fax [phone]
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Di\VIS
FLffi'D LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: PEW-3
Prep Procedure
Analytical Prep Procedures:
BNA SEMIVOLATILES
DOWTHERM
Method
SWB46 35008
SW846 35008
NC Certification Number: 25
Project Number: 60885.00
Report Date August 11, 1999
Page 4 of 4
sample ID L99072310-19
Analyst Prep Date
JMT 07/27/99 0830
JMT 07/27/99 0830
000045
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAVIS
FLffYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: PEW-1
Parameter
Field Data
EPA 170.1
TEMPERATURB
SW846 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Semivolatile Organics
SW846 8270C
1, 2, 4 -TRICHLOROBENZBNE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2, 4-DICHLOROPHENOL
2,4-DIMETHYLPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-METHYL-4,6-DINITROPHENOL
2-METHYLNAPHTHALENE
2-METHYLPHENOL
2-NITROANILINE
2-NITROPHENOL
GW/ChemW
3, 3' -DICJ-ILOROBENZTDINE
3-NITROANILINB
4-BROMOPHENYL PHENYL ETHER
4-CHLOR0-3-METHYLPHENOL
4-CIILOROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-METHYLPHENOL
4-NITROANILINE
4-NITROPJ-IENOT,
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
NC Certification Number: 25
Project Number: 60885.00
Report Date Augu:::t 11, 1999
Page 1 of 4
sample ID L99072310-20
Date Collected: 22-JUL-99 16 :55
Date Received 23-JUL-99
Result RDL Units Analyst Date Time
21. 0 1.0 degreeo C 07/22/99 1655
5. 9 . 0.50 SU 07/22/99 1655
55.0 1.0 utnhoo/cm 07/22/99 1655
801,62 . 01 feet MSL 07/22/99 1655
' 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1417
' 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1417
' 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1417
' 0. 010 0. 010 mg/1 JRN/DSD 08/03/99 1417
' 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1417
' 0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1417
' 0.010 0.010 mg/1 JRN/DSD 08/03/99 1417
' 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1417
' 0.025 0.025 mg/1 JRN/DSD 08/03/99 1417
' 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1417
' 0.010 0. 010 mg/1 JRN/DSD 08/03/99 1417
' 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1417
' 0 .010 0. 010 mg/1 JRN/DSD 08/03/99 1417
' 0 . 025 0 .025 mg/1 JRN/DSD 08/03/99 1417
' 0.010 0.010 mg/1 JRN/DSD 08/03/99 1417
' 0.010 0.010 mg/1 JRN/DSD 08/03/99 1417
' 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1417
' 0.010 0.010 mg/1 JRN/DSD 08/03/99 1417
' 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1417
' 0. 010 0. 010 mg/1 JRN/DSD 08/03/99 1417
' 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1417
' 0. 010 o. 010 mg/1 JRN/DSD 08/03/99 1417
' 0.010 0.010 mg/1 JRN/DSD 08/03/99 1417
' 0 .010 0. 010 mg/1 JRN/DSD 08/03/99 1417
' 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1417
' 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1417
' 0.025 0 . 025 mg/1 JRN/DSD 08/03/99 1417
' 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1417
' 0. 010 0.010 mg/1 JRN/DSD 08/03/99 141 7
' 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1417
000046
Davis & rloyd, Inc. I l'0 Drawer 42B I Greenwood, SC 2<J(>48 I Hl 6 L Durst Avenue I Greenwood, SC 2%49 I [phone] I Fax (8(,4) 229-7119
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Di\VIS
FLtrYD LABORATORY ANALYSIS REPORT
NC Certification Number: 25
Client TICONA,LLC Project Number: 60885.00
P.O. BOX 87
SHBLBY, NC 28150 Report Date Auguot 11, 1999
Contact JERRY MCMURRAY Page 2 of 4
Client ID: PEW-1 Sample ID L99072310·20
Parameter Result Qual RDL Units Analyst Date Time
BENZO(A)ANTHRACENE < 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1417
BENZO(A)PYRENE 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1417
BENZO(B)FLUORANTHENE < 0.010 0. 010 mg/1 JRN/DSD 08/03/99 1417
BENZO(G,H,I)PERYLENE < 0.010 0. 010 mg/1 JRN/DSD 08/03/99 1417
BENZO(K)PLUORANTHENE < 0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1417
BENZOIC ACID < 0. 050 0.050 mg/1 JRN/DSD 08/03/99 1417
BENZYL ALCOHOL < 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1417
BIS(2-CHLOROETHOXY)METHANE < 0.010 0.010 mg/1 JRN/DSD 08/03/99 1417
BIS(2-CHLOROETHYL)ETHER < 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1417
BIS(2-CHLOROISOPROPYL)ETHER < 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1417
BIS(2-ETHYLHEXYL)PHTHALATE < 0 .010 0. 010 mg/1 ' JRN/DSD 08/03/99 1417
BUTYL BENZYL PHTHALATE < 0.010 0.010 mg/1 JRN/DSD 08/03/99 1417
CHRYSENE < 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1417
DI-N-BUTYL PHTHALATE < 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1417
DI-N-OCTYL PHTHALATE < 0.010 0.010 mg/1 JRN/DSD 08/03/99 1417
OIBENZ{A,H)ANTHRACENE < 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1417
DIBENZOFURAN < 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1417
DIETHYL PHTHALATE ' 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1417
DIMETHYL PHTHALATE < 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1417
FLUORANTHENE < 0.010 0. 010 mg/1 JRN/DSD 08/03/99 1417
FLUORENE < 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1417
HEXACHLOROBENZENE < 0.010 0.010 mg/1 JRN/DSD 08/03/99 1417
HEXACHLOROBUTADIENE < 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1417
HEXACHLOROCYCLOPENTADIENE < 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1417
HEXACHLOROETHANE < 0.010 0.010 mg/1 JRN/DSD 08/03/99 1417
INDENO(l,2,3-CD)PYRENE < 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1417
ISOPHORONE < 0. 010 0. 010 mg/1 JRN/DSD 08/03/99 1417
N-NITROSOOI-N-PROPYLAMINE < 0.010 0.010 mg/1 JRN/DSD 08/03/99 1417
N-NITROSOOIPHENYLAMINE < 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1417
NAPHTHALENE < 0 .010 0 .010 mg/1 JRN/0S0 08/03/99 1417
NITROBENZENE < 0.010 0. 010 mg/1 JRN/DSD 08/03/99 1417
PENTACHLOROPHENOL < 0.025 0.025 mg/1 JRN/DSD 08/03/99 1417
PHENANTHRENE < 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1417
PHENOL < 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1417
PYRENE < 0. 010 0. 010 mg/1 JRN/DSD 08/03/99 1417
SWB46 8270C OOWTHERM
1, l' -BI PHENYL ' 0 .010 0. 010 mg/1 DSD/JRN 08/06/99 1200
BIPHENYL ETHER < 0 .010 0. 010 mg/1 DSD/JRN 08/06/99 1200
000047
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 l 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLWYD LABORATORY ANALYSIS REPORT
client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: PEW-1
Parameter
Volatile Organics
SWB46 8260B
1, l , 1-TRICHLOROETHAN'E
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROBTHANE
1,1-DICHLOROETHANE
1, 1-DICHLOROETHENE
1,2-DICHLOROETHANE
1, 2-DICHLOROPROPANB
2-BUTANONE
2-HEXANONB
4 -METHYL-2-PENTANONE
ACBTONE
BENZENE
BROMOOICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHl,OROBBNZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CI.C:-1, 2-DICl!LOROBTHBNE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
BTHYLBENZENE
METHYLENE CHLORIDE
NAPHTHALBNE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
'
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NC Certification Number: 25
Project Number: 60885.00
Report Date
Page 3 of 4
Sample ID
AuguDt 11, 1999
L99072310-20
Result Qual RDL Units Analyst Date
0 .0050 0.0050 mg/1 PAP 07/27/99
0 .0050 0.0050 mg/1 PAP 07/27/99
0.0050 0 . 0 050 mg/1 PAP 07/27/99
0.0050 0 .0050 mg/1 PAP 07/27/99
0.0050 0.0050 mg/1 PAP 07/27/99
0.0050 0 .0050 mg/1 PAP 07/27/99
0.0050 0 . 0 050 mg/1 PAP 07/27/99
0.010 0.010 mg/1 PAP 07/27/99
0.010 0.010 mg/1 PAP 007 /27 /99
0.0050 0.0050 mg/1 PAP 07/27/99
0.010 0. 010 mg/1 PAP 07/27/99
0 . 0050 0 . 0050 rng/1 PAP 07/27/99
0 . 0050 0 .0050 mg/1 PAP 07/27/99
0.0050 0.0050 mg/1 PAP 07/27/99
0.010 0.010 rng/1 PAP 07/27/99
0 . 0050 0 . 0050 rng/1 PAP 07/27/99
0.0050 0.0050 mg/1 PAP 07/27/99
0.0050 0.0050 rng/1 PAP 07/27/99
0.010 0.010 rng/1 PAP 07/27/99
0.0050 0.0050 rng/1 PAP 07/27/99
0.010 0. 010 rng/1 PAP 07/27/99
0.0050 0.0050 rng/1 PAP 07/27/99
0 .0050 0.0050 rng/1 PAP 07/27/99
0 . 00 so 0 . 0050 rng/1 PAP 07/27/99
0 .0050 0 .0050 mg/1 PAP 07/27/99
0,0071 0.0050 mg/1 PAP 07/27/99
0 .0050 0.0050 mg/1 PAP 07/27/99
0 .0050 0 .0050 mg/1 PAP 07/27/99
0 . 0050 0 . 0050 mg/1 PAP 07/27/99
0 .0050 0 .0050 mg/1 PAP 07/27/99
0.0050 0.0050 mg/1 PAP 07/27/99
0.0050 0.0050 mg/1 PAP 07/27/99
0.0066 0 .0050 mg/] PAP 07/27/99
0.010 0 .010 mg/1 PAP 07/27/99
0.010 0.010 mg/1 PAP 07/27/99
0.0050 0.0050 mg/1 PAP 07/27/99
000048
Time
1728
l 72 8
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
1728
Davis & Floyd, Inc. I 1'0 Drt1wcr 428 I Greenwood, SC 29(,48 I 81 (, L Durst Avenue I Greenwood, SC 29649 I (B64} 229-4413 I Fax [phone]
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DAYIS
FLl1YD LABORATORY ANALYSIS REPORT
client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: PE:W-1
Prep Procedure
Analytical Prep Procedures:
BNA SEMIVOLATILE3
DOWTHERM
Method
SW846 35008
SWB-46 35008
NC Certification Number: 25
Project Number: 60885.00
Report Date Auguot 11, 1999
Page 4 of 4
Sample ID L99072310-20
Analyst Prep Date
JMT 07/27/99 0830
JMT 07/27/99 0830
00004!:l
Davis & Floyd, Inc. I PO Drawer 42H I Greenwood, SC 29(>48 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLbYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: F-55
Parameter
Field Data
EPA 170.1
TEMPERATURE
SW846 9040B
PH
SW846 9050
Matrix
SPECIPIC CONDUCTIVITY
GROUND WATER ELEVATION
Somivola.tile Organics
SW846 8270C
1, 2, 4 -TRICHLOROBENZENE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DICHLOROPHENOL
2,4-DIMETHYLPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-METHYL-4,6-DINfTROPHENOL
2-METHYLNAPHTHALENE
2-METHYLPHENOL
2-NITROANILINE
2-NITROPHENOL
3,3'-DICHLOROBENZIDINE
3-NITROANILINE
4-BROMOP!-!ENYL PHENYL ETHER
4-CHLOR0-3-METHYLPHENOL
4-CHLOROANILINE
GW/ChemW
4-CHLOROPHENYL PHENYL ETHER
4-METHYLPHENOL
4-NITROANILINE
4-NITROPHF.NOL
ACENAPHTHENE
ACBNAPHTJ-IYLENE
ANTHRACENE
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NC Certification Number: 25
Project Number: 60885.00
Report Date August 11, 1999
Page 1 of 4
Sample ID L99072310-21
Date Collect,;,d: 22-JUL-99 1 7: 14
Date Received 23-JUL-99
Reault Qua.l RDL Units Analyst Date Time
22.0 1. 0 degree□ C 07 /22/99 1714
6.5 0.50 OU 07/22/99 1714
327 1.0 umhon/cm 07 /22/99 1714
810.93 feet MSL 07/22/99 1714
0 .010 0. 010 mg/1 JRN/DSD 08/03/99 1455
0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1455
0 .010 0.010 mg/1 JRN/DSD 08/03/99 1455
0. 010 0. 010 mg/1 JRN/DSD 08/03/99 1455
0. 010 0 -010 mg/1 JRN/DSD 08/03/99 1455
0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1455
0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1455
0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1455
0. 025 0.025 mg/1 JRN/DSD 08/03/99 1455
0.010 0.010 mg/1 JRN/DSD 08/03/99 1455
0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1455
0.010 0. 010 mg/1 JRN/DSD 08/03/99 1455
0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1455
0.025 0. 025 mg/1 JRN/DSD 08/03/99 1455
0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1455
0 .010 0.010 mg/1 JRN/DSD 08/03/99 1455
0.010 0. 010 mg/1 JRN/DSD 08/03/99 1455
0.010 0. 010 mg/1 JRN/DSD 08/03/99 1455
0 .010 0.010 mg/1 JRN/DSD 08/03/99 1455
0.010 0. 010 mg/1 JRN/DSD 08/03/99 1455
0 .010 .010 mg/1 JRN/DsD 08/03/99 1455
0.010 0. 010 mg/1 JRN/DSD 08/03/99 1455
0.010 0. 010 mg/1 JRN/DSD 08/03/99 1455
0 .010 0.010 mg/1 JRN/DSD 08/03/99 1455
0.12 0.050 mg/1 JRN/DSD 08/03/99 1728
0.010 0.010 mg/1 JRN/DSO 08/03/99 1455
0. 025 0.025 mg/1 JRN/DSD 08/03/99 1455
0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1455
0.010 0.010 mg/1 JRN/DSO 08/03/99 1455
0. 010 0. 010 mg/1 JRN/DSD 08/03/99 14 55
000050 Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 j 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-441] I Fax [phone]
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D~S I LABORATORY ANALYSIS REPORT FL D
I NC Certification Number: 25
I Client TICONA,LLC Project Number: 60885.00
P.O. BOX 87
SHELBY, NC 28150 Report Date Augunt 11, 1999
I Contact JERRY MCMURRAY Page 2 of 4
Client ID: F-55 Sample ID L99072310-21
I Parameter Reisult Qual RDL Uni ta Analyst Date Tim■
BENZO(A)ANTHRACENE ' 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1455
BENZO (A} PYRENE ' 0 .010 0.010 mg/1 JRN/DSD os/03/99 1455 I BENZO(B)FLUORANTHENE ' 0 . 010 0 . 010 mg/1 JRN/DSD 08/03/99 1455
BENZO(G,H,I)PERYLENE ' 0. 010 0.010 mg/1 JRN/DSD OB/03/99 14 55
BENZO(K)FLUORANTHENE ' 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1455
I BENZOIC ACID ' 0. 050 0.050 mg/1 JRN/DSD 08/03/99 1455
BENZYL ALCOHOL ' 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1455
BIS(2-CHLOROETHOXY)METHANE ' 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1455
BIS(2-CHLOROETHYL)ETHER ' 0.010 0.010 mg/1 JRN/DSD 08/03/99 1455
I 8IS(2-CHLOROISOPROPYL)ETHER ' 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1455
BIS (2-ETHYLHEXYL) PHTHALATE < 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1455
BUTYL BENZYL PHTHALATE < 0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1455
CHRYSENE ' 0.010 0.010 mg/1 JRN/DSD 08/03/99 1455 I D1-N-BUTYL PHTHALATE < 0.010 0. 010 mg/1 JRN/DSD 08/03/99 1455
DI-N-OCTYL PHTHALATE ' 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1455
DIBENZ(A,H)ANTHRACENE ' 0.010 0. 010 mg/1 JRN/DSDJ08/03/99 1455
I DIBENZOFURAN 0.036 0 .010 mg/1 JRN/DSD 08/03/99 14 55
DIETHYL PHTHALATE ' 0.010 0. 010 mg/1 JRN/DSD 08/03/99 1455
DIMETHYL PHTHALATE ' 0.010 0.010 mg/1 JRN/DSD 08/03/99 1455
FLUORANTHENE ' 0.010 0.010 mg/1 JRN/DSD 08/03/99 1455
I FLUORENE ' 0. 010 0. 010 mg/1 JRN/DSD 08/03/99 1455
HEXACHLOROBENZENE ' 0.010 0. 010 mg/1 JRN/DSD 08/03/99 14 55
HEXACHLOROBUTADIENE < 0. 010 0.010 mg/1 JRN/DSD 08/03/99 1455
HEXACHLOROCYCLOPENTADIENE ' 0 .010 0. 010 mg/1 JRN/DSD 08/03/99 1455
I HEXACHLOROETHANE ' 0 .010 0 .010 mg/1 JRN/DSD 08/03/99 1455
INDENO(l,2,3-CD)PYRENE ' 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1-455
ISOPHORONE ' 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1455
N-NITROSODI-N-PROPYLAMINE < 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1455 I N-NITROSODIPHENYLAMINE < 0 .010 0.010 mg/1 JRN/DSD 08/03/99 1455
NAPHTHALENE 0.33 0 .050 mg/1 JRN/DSD 08/03/99 1728
NITROBENZENE ' 0.010 0 .010 mg/1 JRN/DSD 08/03/99 1455
I PENTACHLOROPHENOL ' 0. 025 0.025 mg/1 JRN/DSD 08/03/99 1455
PHENANTHRENE ' 0. 010 0 .010 mg/1 JRN/DSD 08/03/99 1455
PHENOL 0. 033 0 .010 mg/1 JRN/DSD 08/03/99 1455
PYRENE ' 0.010 0. 010 mg/1 JRN/DSD 08/03/99 1455
I SW846 8270C DOWT'HERM
1, l' -BI PHENYL 12.4 1. 0 rng/1 DSD/JRN 08/06/99 1541
BIPHENYL ETHER 35.4 4.0 mg/1 DSD/JRN 08/06/99 1655
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000051
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DA,YIS
FLtfYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX B7
SHELBY, NC 28150
JERRY MCMURRAY
client ID: F-55
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1, 2 -DIC!-ILOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENH
B ROMO□ I CH LOR OM ETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULPIDB
CARBON TETR~CHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1, 2-DICHLOROBTHENE
CIS-1, 3 -DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETl!ENH
TOLUENE
TRANS~l,2-DICHLOROETHENE
TRANS-1,J-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
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NC Certification Number: 25
Project Number: 60885.00
Report Date
Page 3 of 4
Sample ID
Auguot 11, 1999
L99072310-21
Result Qual RDL Units Analyst Date
0 .0050 '. 0050 mg/1 PAP 07/28/99
0 .0050 0 .0050 mg/1 PAP 07/28/99
0 .0050 0 .0050 mg/1 PAP 07/28/99
0.0050 0.0050 mg/1 PAP 07/28/99
0 .0050 0.0050 mg/1 PAP 07/28/99
0.0050 0 .0050 mg/1 PAP 07/28/')9
0.0050 0.0050 mg/1 PAP 07/28/99
0 .010 0. 010 mg/1 PAP 07/28/99
0.010 0.010 mg/1 PAP 07/28/99
0.0050 0.0050 mg/1 PAP 07/28/99
0.010 0. 010 mg/1 PAP 07/28/99
0. 053 0.0050 mg/1 PAP 07/28/99
0 . 0050 0 . 0050 mg/1 PAP 07/28/99
0.0050 0.0050 mg/1 PAP 07/28/99
0. 010 0.010 mg/1 PAP 07/28/99
0.0050 0.0050 mg/1 PAP 07/28/99
0 .0050 0 .0050 mg/1 PAP 07/28/99
0.0050 0.0050 mg/1 PAP 07/28/99
0.010 o. 010 mg/1 PAP 07/28/99
0.0050 0.0050 mg/1 PAP 07/28/99
0. 010 0.010 mg/1 PAP 07/28/99
0 .0050 0.0050 mg/1 PAP 07/28/99
0.0050 0.0050 mg/1 PAP 07/28/99
0.0050 0.0050 mg/1 PAP 07/28/99
0.0050 0 . 0050 mg/1 PAP 07/28/99
0.013 0.0050 mg/1 PAP 07/28/99
0 .0050 0.0050 mg/1 PAP 07/28/99
0 .0050 0.0050 mg/1 PAP 07/28/99
0.0050 0 .0050 mg/1 PAP 07/28/99
0 .0050 0.0050 mg/1 PAP 07/28/99
0. 0050 0.0050 mg/1 PAP 07/28/99
0.0050 0.0050 mg/1 PAP 07/28/99
0 .010 0 .010 mg/1 PAP 07/28/99
0 .010 0 .010 mg/1 PAP 07 /28/99
0.0050 0.0050 mg/1 PAP 07/28/99
000052
Time
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
0915
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue l Greenwood, SC 29649 I [phone] I Fax (8fi4) 229-7119
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DAYIS
FLbYD LABORATORY ANALYSIS REPORT
client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: F-55
Prep Procedure
Analytical Prep Procedures:
BNA SEMIVOLATILES
DOWTHERM .
Method
SW846 35008
SW846 3500B
NC Certification Number: 25
Project Number: 60885.00
Report Date Auguot 11, 1999
Page 4 of 4
Sample ID L99072310-21
Analyst Prep Date
JMT 07/27/99 0830
JMT 07/27/99 0830
000053
Davis & Floyd, Inc. 1 PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue l Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLi1YD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: TRIP BLANK
Mat.rix
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BR OMO FORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1, 2-DICIILOROETHENB
CIS-1,3-DICHLOROPROPBNB
DIBROMOCHLOROMETHANE
BTHYLBENZBNB
MBTHYLENE CHLORIDE
STYRENE
TETRACHLOROETl-!ENB
TOLUENB
TRANS-1,2-DICHLOROETHBNB
TRANS-1,3-DICHLOROPROPENB
TRICHLOROETHENE
VINYL ACBTATE
VINYL CHLORIDE
XYLENB (TOTAL)
GW/ChemW
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NC Certification Number: 25
Project Number: 60885.00
Report Date Augm;t 11, 1999
Page 1 of 1
Sample ID L99072310-22
Date Collected: 21-JUL-99 06 ; 30
Date Received ' 23-JUL-99
Result Qual RDL Units Analyst Date Time
0.0050 0.0050 mg/1 PAP 07/28/99 1158
0.0050 o. 0050 mg/1 PAP 07/28/99 1158
0.0050 0 .0050 mg/1 PAP 07/28/99 1158
0 .0050 0 .0050 mg/1 PAP 07/28/99 1158
0.0050 0 .0050 mg/1 PAP 07/28/99 1158
0.0050 0 .0050 mg/1 PAP 07/28/99 1158
0.0050 0 . 0050 mg/1 PAP 07/28/99 1158
0 .010 0. 010 mg/1 PAP 07/28/99 1158
0.010 0. 010 mg/1 PAP 07/28/99 1158
0.0050 0.0050 mg/1 PAP 07/28/99 1158
0. 010 0. 010 mg/1 PAP 07/28/99 1158
0.0050 0.0050 mg/1 PAP 07/28/99 1158
0 .0050 0.0050 mg/1 PAP 07/28/99 1158
0.0050 0 .0050 mg/1 PAP 07/28/99 1158
0. 010 0.010 mg/1 PAP 07/28/99 1158
0.0050 0.0050 mg/1 PAP 07/28/99 1158
0.0050 0. 0050 mg/1 PAP 07/28/99 1158
0.0050 0 .0050 mg/1 PAP 07/28/99 1158
0.010 0.010 mg/1 PAP 07/28/99 1158
0.0050 0.0050 mg/1 PAP 07/28/99 1158
0.010 0. 010 mg/1 PAP 07/28/99 1158
0 . 0050 0 .0050 mg/1 PAP 07/28/99 1158
0 .0050 0.0050 mg/1 PAP 07/28/99 1158
0 . 0050 0.0050 mg/1 PAP 07/28/99 1158
0 . 0050 0 .0050 mg/1 PAP 07/28/99 1158
0 . 0050 0.0050 mg/1 PAP 07/28/99 1158
0.0050 0 .0050 mg/1 PAP 07/28/99 1158
0.0050 0.0050 mg/1 PAP 07/28/99 1158
0.0050 0 .0050 mg/1 PAP 07 /28/99 1158
0 .0050 0.0050 mg/1 PAP 07/28/99 1158
0 .0050 0 .0050 mg/1 PAP 07/28/99 1158
0.0050 0.0050 mg/1 PAP 07/28/99 1158
0.010 0. 010 mg/1 PAP 07/28/99 1158
0. 010 0 .010 mg/1 PAP 07/28/99 1158
0.0050 0.0050 mg/1 PAP 07/28/99 1158
000054
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (8b4) 229-4413 I Fax (H64) 229-7119
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o~i•s
FLOYD LABORATORY ANALYSIS REPORT
Master Tracking List
Sample ID
L99072310-01
Field Data
EPA 170.1
SW846 904GB
SW846 9050
Client
Contact
Volatile Organice
SWB46 8260B
L99072310-02
Field Data
EPA 170.l
SWB46 9040B
SW846 9050
Volatile Organics
SW846 8260B
L99072310-03
Field Data
EPA .170 . .I
SW846 9040B
SW846 9050
Oas Chromatography
SW846 8015
Volatile organics
SW846 8260B
Wet Chemistry
SW846 9060
L99072310-04
Field Data
EPA 170 . .l
SW846 9040B
SWB46 9050
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID
HH-48
ITCI
C-49
NC Certification Number: 25
Project Number: 60885.00
Report Date Augunt 11, 1999
Page 1 of 7
Date Collected Date R•ceived
21-JUL-99 12:07 23-JUL-99
07/21/99 1200
07/21/99 12 00
07/21/99 1200
07 /27 /99 0953
21-JUL-99 12:07 23-JUL-99
07/21/99 1206
07/21/99 1206
07/21/99 1206
07/27/99 1013
21-JUL-99 12:07 23-JtTL-99
07/21/99 1250
07/21/99 12 50
07/21/99 12 50
08/02/99 1712
07/27/99 1034
07/26/99 1132
21-JUL-99 14: 07 23-JUL-99
07/21/99 1419
07/21/99 1419
07/21/99 1419
000055
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] \ Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Master Tracking List
Client
Contnct.
Sample ID
Volatile organics
SW846 8260B
L99072310-05
Field Data
EPA 170 .1
SW846 9040B
SWB46 9050
Volatile Organics
SW846 8260B
L99072310-06
Field Data
EPA 170.1
SWB46 9040B
SW846 9050
Volatile Organica
SWB46 8260B
L99072310-07
Field Data
EPA 170.1
SW846 9040B
SW84G 9050
Volatile Organico
SW846 8260B
L99072310-08
Field Data
EPA 170.l
SW846 9040B
SW846 9050
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
J8RRY MCMURRAY
client ID
T-35
EE-58
FF-34
NC Certification Number: 25
Project Number: 60885.00
Report Date
Page 2 of 7
Augll!lt 11, 1999
Date Collected
21-JUL-99 15:07
21-JUL-99 16:07
21-JUL-99 17:07
000056
Date Received
07 /27 /99 1054
23-JUL-99
07/21/99 1526
07/21/99 1526
07/21/99 1526
07/27/99 1114
23-JUL-99
07/21/99 1611
07 /21/99 1611
07/21/99 1611
07/27/99 1135
23-JUL-99
07/21/99 1716
07/21/99 1716
07/21/99 1716
07 /27 /99 1155
07/21/99 1725
07/21/99 1725
07/21/99 1725
Davis & Floyd, Inc. I 1'0 Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue ] Greenwood, SC 29(,49 I [phone] I Fax [phone]
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
NC Certification Number: 25
Master Tracking List
Client TICONA,LLC Project Number: 60885.00
P.O. BOX B7
SHELBY, NC 2 8150 Report Date Augu~t 11, 1999
Contact JERRY MCMURRAY Page 3 of 7
Sampla ID Client ID Data Collected Date Received
Volatile Organics
SWB46 8260B 07/27/99 1216
L99072310-09 GG-61 22-JOL-99 10: 07 23-JOL-H
Field Data
EPA 170. l 07/22/99 1017
SW846 9040B 07/22/99 1017
SWB46 9050 07/22/99 1017
Volatile Organics
SW846 8260B 07/27/99 123 6
L990723l0-10 AA-54 22-JUL-99 10; 07 23-JUL-99
Field Data
EPA 170. 1 07/22/99 1058
SW846 904GB 07/22/99 1058
SW846 9050 07/22/99 1058
Volatile Organics
SW846 82608 07/27/99 1257
L99072310-11 P-58 22-JUL-99 12: 07 23-JUL-99
Field Data
EPA 170. 1 07/22/99 1205
SW846 9040B 07/22/99 1205
SW846 9050 07 /22/99 1205
Volatile Organics
SW846 8260B 07 /27 /99 1422
L99072310-12 ITEF 22-JUL-99 12: 07 23-JUL-99
Field Data
EPA 170. l 07/22/99 1230
SW846 9040B 07/22/99 1230
SW846 9050 07 /22/99 123 0
000057
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I lll 6 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
NC Certification Number: 25
Master Tracking List
Client
Contact
Sample ID
Oas Chromatography
SW846 8015
Volatile Organics
SW846 8260B
Wet Chemistry
SW846 9060
L99072310-13
Field Data
EPA 170.
SW846 9040B
SW846 9050
Gae chromatography
SW846 8015
Volatile Organics
SWB46 8260B
Wet Chemistry
SW846 9060
L99D72310-14
Field Data
EPA 170.1
SW846 9040B
SW846 9050
Volatile Organics
SW846 8260B
Wet Chemiotry
SW846 9060
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID
ITEF DUP.
K-28
Project Number: 60885.00
Report. Date
Page 4 of 7
Augu□t 11, 1999
Date Collected
22-JUL-99 12:07
22-JUL-99 13:07
000058
Date Receivod
08/02/99 1226
07/27/99 1443
07/26/99 1149
23-JUL-99
07/22/99 1230
07/22/99 1230
07/22/99 1230
08/02/99 1249
07/27/99 1503
07 /26/99 1330
23-JUL-99
07/22/99 1320
07/22/99 1320
07/22/99 1320
07/27/99 1524
07/26/99 1349
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 ! 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] ! Fax [phone]
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LABORATORY ANALYSIS REPORT
Master Tracking List
Sample ID
L99072310-15
Fiald Data
EPA 170.1
SW846 90408
SWB46 9050
Client
Contact
Volatile Organice
SW846 8260B
Wet Chemistry
SWB46 9060
L99072310-16
Field Data
EPA 170.1
SW846 9040B
SW846 9050
Volatile Organics
SW846 8260B
L99072310-17
Field Data
EPA 170.1
SW846 9040B
SW846 9050
Semivolatile organics
SW846 8270C
SW846 8270C DOWTHERM
Volatile Organice
SW846 8260B
L99072310-19
Field Data
EPA .170.1
SWB46 9040B
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID
V-23
CC-33
PEW-4
PEW--4 DUP.
NC Certification Number: 25
Project Number: 60885.00
Report Date Auguot 11, 1999
Page 5 of 7
Date Collected Date Received
.!2-JUL-99 13: 07 23-JOL-99
07/22/99 13 5 7
07/22/99 1357
07/22/99 1357
07/27/99 1849
07/26/99 1410
22-JUL-99 14: 07 23-JUL-99
07/22/99 1427
07/22/99 142 7
07/22/99 1427
07/27/99 1605
22-JUL-99 15: 07 23-JUL-99
07/22/99 1515
07/22/99 1515
07/22/99 1515
08/03/99 1222
08/06/99 1 01, 1
07/27/99 1626
22-JUL-99 15: 07 23-JUL-99
07/22/99 1515
07/22/99 1515
00005~l
Davis & Floyd, Inc. I PO Drawer 42B I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] \ Fax [phone]
DAVIS
FLifYD LABORATORY ANALYSIS REPORT
Master Tracking List
Client
Co11tact
Sample ID
SW846 9050
Semivolatile Organics
SW846 8270C
SW846 8270C DOWTHERM
Volatile Organics
SW846 8260B
L99072310-H
Field Data
EPA 170 .1
SW846 9040B
SW846 9050
Semivolatile Organics
SW846 8270C
SW846 8270C DOWTHERM
Volatile Organics
SWB46 8260B
L99072310-20
Field Data
EPA 170.1
SW846 9040B
SW846 9050
Semivolatile Organics
SWB46 8270C
SW846 8270C DOWTHERM
Volatile Organics
SW846 8260B
L99072310-21
Field Data
EPA 170. l
SW846 9010B
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID
PEW-3
F-55
NC Certification Number: 25
Project Number: 60885.00
Report Date Auguot 11, 1999
Page 6 of 7
Date Collected Date Received
07/22/99 1515
08/03/99 1300
08/06/99 1048
07/27/99 1647
22-JUL-99 16: 07 23-JUL-99
07/22/99 1624
07/22/99 1624
07/22/99 1624
08/03/99 1339
08/06/99 1124
07/27/99 1707
22-JUL-99 16:07 23-JOL-99
07 /22/99 1655
07/22/99 1655
07/22/99 1655
08/03/99 1417
08/06/99 12 00
07/27/99 1728
22-JUL-99 17 :07 23-JUL-99
07/22/99 1714
07/22/99 1714
000060
Davis & rloyd, Inc. I PO Drawer 42B I Greenwood, SC 2'.)648 I 81 (1 F.. Durst Avenue I Greenwood, SC 29649 I (/:1(14) 229-4413 I Fax (Hf14) 229-7119
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DAYIS
FL(j\7D LABORATORY ANALYSIS REPORT
Master Tracking List
Client TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
Contact JERRY MCMURRAY
Sample ID
SW846 9050
Semivolatile Organics
SW846 8270(.'
SW846 8270C DOWTHERM
Volatile Organics
SW846 8260B
L990723l.0-22
Volatile Organics
SW846 8260B
Client ID
TRIP BLANK
NC Certification Number: 25
Project Number: 60885.00
Report Date
Page 7 of 7
AuguGt 11, 1999
Data Collected
21-JUL-99 06:07
000061
Date Received
07/22/99 1714
08/03/99 1455
08/06/99 1541
07/28/99 0.915
23-JUL-99
07 /28/99 1158
Davis & r-loyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 81(, E. Durst Avenue I Greenwood, SC 2%49 I [phone] I Fax [phone]
DAYIS
FLtwD LABORATORY ANALYSIS REPORT
Method Coriformance Summary
Client: HNA HOLDINGS, INC.
Login: L99072310
Criteria Volatiles
Sample Holding Time
Standards Preparation
Instrument Tuning
Instrument Calibration
Calibration Verification
Degradation Check
. Interference
Sample/Standard
B Ian ks Resu Its
Method Accuracy
Method Precision
Surrogate Recovery
PDS/SD/MSA
TCLP Preparation
✓
NIA
Met Criteria Met
Not Applicable
'i
'i
'i
'i
'i
NIA
NIA
'i
•
'i
'i
NIA
NIA
Semi
Volatiles
✓
✓
✓
✓
✓
NIA
NIA
✓
✓
✓
✓
NIA
NIA
Metals
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
*
PDS =
SD =
MSA=
Method Criteria Not Met -See footnote(s) below.
Post Digestion Spike
Serial Dilution
Method of Standard Additions
Footnotes: TOC is summarized under "Inorganics" column.
Ethylene glycol is summarized under "Other" column.
Project Number: 60885.00-0000
Report Date: August 11, 1999
Inorganics Other
'i •
'i ✓'
NIA NIA
✓ 'i
✓ 'i
NIA NIA
NIA NIA
'i 'i
'i 'i
'i 'i
NIA NIA
NIA NIA
NIA NIA
Ethylene glycol analyses were perforrned 12 days after sample collection. Although
not specifically listed, ethylene glycol is analyzed adhering the procedure stated
in SW-846 Method 8015. The analyses exceed that holding time by 5 days.
Prepared
1 The continuing calibration standard reference number indicated in the analyses log
represents that of the I 0000 mg/L stock solution and not 50 mg/L. The
preparation appears to be correct based upon the instrument response (42.98
mg/L).
A total 5 out of 10 sample spike compounds recovered slightly below the laboratory-
established limits in the MS and MSD perforrned on sample L990723 IO-IO (AA-
54 ). The associate LCS met all recovery requirements.
00006'.1
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Davis & cloyd, Inc. I 1'0 Drawer 428 I Greenwood, SC 2%48 I 81 r.E. Durst Avenue I Greenwood, SC 29(,49 I (864) 229-44 IJ I Fax [phone] I
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DA,YIS
FLOYD LABORATORY ANALYSIS REPORT
Surrogates % Recovery
L99D72310-01 27-JUL-99 09:53
L99072310-02 27-JUL-99 10; 13
L99072310-03 27-JUL-99 10 : 34
L99072310-04 27-JUL-99 10 : 54
L99072310-05 27-JUL-99 11 :14
L99072310-06 27-JUL-99 11 ; 35
L99072310-07 27-JUL-99 11 ;55
L99072310-0B 27-JUL-99 12 ; 16
L99072310-09 27-JUL-99 12 : 3 6
L99072310-10 27-JUL-99 12 :57
L99072310-11 27-JUL-99 14:22
L99072310-12 27-JUL-99 14 : 43
L99072310-13 27-JUL-99 15: 0)
L99072310-14 27-JUL-99 15 : 24
L99072310-15 27-JUL-99 18 : 49
L99072310-16 27-JUL-99 16: 05
L99072310-17 27-JUL-99 16 : 26
L99072310-18 27-JUL-99 16 : 47
L99072310-19 27-JUL-99 17: 07
L99072310-20 27-JUL-99 17 : 28
L99072310-21 28-JUL-99 09: 15
L99072310-22 2B-JUL-99 11 :58
LCS1B385:1 27-JUL-99 18 :08
MB18385:l 27-JUL-99 09 : 30
MS99072310-10 :183B5 27-JUL-99 1) : 17
MSD99072310-10: 18385 27-JUL-99 13 : 41
LCS18386:1 28-JUL-99 10 : 3 6
MB18386:1 28-JUL-99 08 :12
MS99072310-21 :18386 28-JUL-99 09 : 35
MSD99072310-21:18386 28-JUL-99 09: 56
DCB 1,2-DICHLOROETHANE-D4
BFB BROMOFLUOROBENZENE
TDL TOLUENE-OS
98.8
101. 6
102.8
102 .5
102. 5
102.5
101. 3
102.9
103.9
99.9
101. 8
107 . '
107 . 8
110 .7
101. 1
106. 2
109 .2
109. 3
105 .7
10) .o
100. 8
98.6
105. 8
108 . J
106.2
107 .)
104 . 2
104.4
102. 2
107. 7
88.2
86.6
92.1
86.1
87 . 9
8) .5
81 . 2
82.3
84.4
85.1
85.5
86.9
86.4
89.9
102 .1
90.8
82.7
87 . 8
88 .6
86 .0
102.2
8) . 4
82 .,
87 .o
90 . 4
87 . 0
92 . 6
86 .2
108 . 5
107 . 5
Report Date
Page 1 of 1
Matrix
Method
104.8
106.8
102.3
10) . 6
104 . 8
105 . J
107 .)
105. 4
105. 7
106. 4
104.6
104 . 2
104 .6
102 . 8
100.
104 . 2
10) . 5
102 . 0
103 .4
105. 0
98.5
106 . 5
106 .0
102 .8
101 . 6
102 . )
10) . 0
10) .)
96 .5
95. )
000061
Augunt 11, 1999
GW/ChemW
SW846 8260
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2%48 I 816 E. Durst Avenue I Greenwood, SC 29649 I (ll(i4) 229-4413 I Fax (Bb4) 229-7119
DA,YIS
FLtwD
Method Blanks
Bl<mk
Parameter
Volatile Organico
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1, 1, 2 -TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETflENE
1,2-DICHLOROETl!ANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMBTHANE
CIS-1, 2-DICHLOROETHENH
CIS-1, 3-DICHLOROPROPENE
DIBROMOCHLOROMBTHANE
ETHYLBENZENE
METHYLENE CHLORIDE
NAf'HTHALENE
STYRENE
TETRACHLOROETHENE
TOLUENE:
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
MB18J85:l
LABORATORY ANALYSIS REPORT
Cone
' 5.0
' 5.0
' 5.0
' 5 . 0
' 5.0
' 5.0
' 5.0
' 10.0
' 10.0
' 5.0
' 10.0
' 5 .0
' 5.0
' 5.0
' 10 . 0
' 5.0
' 5.0
' 5.0
' 10.0
' 5.0
' 10.0
' 5 . 0
' 5 . 0
' 5.0
' 5.0
' 5. 0
' 5. 0
' 5.0
' 5.0
' 5. 0
' 5.0
' 5.0
' 5.0
' 10.0
' 10.0
' 5 .0
000064
Report Date
Page 1 of l
Auguot 11, 1999
Matrix GW/ChernW
WorkGroup: WG18385
Qual RDL Units Analyst Date
5.0 ug/1 PAP 07/27/99
5.0 ug/1 PAP 07/27/99
5.0 ug/1 PAP 07/27/99
5 . 0 ug/1 PAP 07/27/99
5. 0 ug/1 PAP 07/27/99
5. 0 ug/1 PAP 07/27/99
5.0 ug/1 PAP 07/27/99
10. 0 ug/1 PAP 07/27/99
10.0 ug/1 PAP 07/27/99
5. 0 ug/1 PAP 07/27/99
10. 0 ug/1 PAP 07/27/99
5. 0 ug/1 PAP 07/27/99
5 . 0 ug/1 PAP 07/27/99
5.0 ug/1 PAP 07/27/99
10 . 0 ug/1 PAP 07/27/99
5.0 ug/1 PAP 07 /27 /99
5.0 ug/1 PAP 07/27/99
5.0 ug/1 PAP 07/27/99
10.0 ug/1 PAP 07/27/99
5. 0 ug/1 PAP 07/27/99
10.0 ug/1 PAP 07/27/99
5 .o ug/1 PAP 07/27/99
5 . 0 ug/1 PAP 07/27/99
5.0 ug/1 PAP 07/27/99
5 . 0 ug/1 PAP 07/27/99
5.0 ug/1 PAP 07/27/99
5.0 ug/1 PAP 07/27/99
5.0 ug/1 PAP 07/27/99
5 .0 ug/1 PAP 07/27/99
5.0 ug/1 PAP 07/27/99
5.0 ug/1 PAP 07/27/99
5.0 ug/1 PAP 07/27/99
5. 0 ug/1 PAP 07/27/99
10.0 ug/1 PAP 07/27/99
10 . 0 ug/1 PAP 07/27/99
5.0 ug/1 PAP 07/27/99
Time
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
0930
Davis & r-loyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 81(i 1:. Durst Avenue I Greenwood, SC 29649 ! [phone] I Fax {8(i4) 229-7119
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Df\YIS
FLtJ\'D
Method Blanks
Blank
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TBTRACHLOROETHANB
1,1,2-TRICHLOROETHANE
1,1-DICHLOROBTHANB
1,1-DICHLOROETHBNB
1,2-DICHLOROBTHANE
1,2-0ICHLOROPROPANE
2-BUTANONB
2-HEXANONB
4-MBTHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANB
BROMOFORM
BROMOMETHANB
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBBNZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANB
CIS-1, 2 -DICJ-ILOROBTHENE
CIS-1,3-DICHLOROPROPBNE
DIBROMOCHLOROMBTHANE
BTHYLBBNZBNE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHBNE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
MB18386:1
LABORATORY ANALYSIS REPORT
Report Date August 11, 1999
Page 1 of 1
Matrix GW/Chemw
WorkGroup: WG18386
Cone Qual RDL Units Analyst Date Time
< 5. 0 5.0 ug/1 PAP 07/28/99 0812
< 5.0 5.0 ug/1 PAP 07/28/99 0812
< 5.0 5.0 ug/1 PAP 07 /28/99 0812
< 5.0 5.0 ug/1 PAP 07/28/99 0812
< 5.0 5.0 ug/1 PAP 07/28/99 0812
< 5.0 5.0 ug/1 PAP 07/28/99 0812
< 5.0 5.0 ug/1 PAP 07 /28/99 0812
< 10.0 10. 0 ug/1 PAP 07/28/99 0812
< 10 .0 10 .0 ug/1 PAP 07/28/99 0812
< 5. 0 5.0 ug/1 PAP 07/28/99 0812
< 10.0 10.0 ug/1 PAP 07/28/99 0812
< 5.0 5. 0 ug/1 PAP 07/28/99 0812
< 5.0 5.0 ug/1 PAP 07/28/99 0812
< 5.0 5. 0 ug/1 PAP 07/28/99 0812
< 10.0 10 .0 ug/1 PAP 07/28/99 0812
< 5.0 5 .0 ug/1 PAP 07/28/99 0812
< 5 .o 5.0 ug/1 PAP 07/28/99 0812
< 5 .0 5.0 ug/1 PAP 07 /28/99 0812
< 10.0 10.0 ug/1 PAP 07/28/99 0812
< 5. 0 5.0 ug/1 PAP 07/28/99 0812
< 10.0 10 . 0 ug/1 PAP 07/28/99 0812
< 5. 0 5. 0 ug/1 PAP 07/28/99 0812
< 5.0 5.0 ug/1 PAP 07/28/99 081.2
< 5.0 5.0 ug/1 PAP 07/28/99 0812
< 5 .0 5.0 ug/1 PAP 07/28/99 0812
< 5 .0 5 . 0 ug/1 PAP 07/28/99 0812
< 5.0 5.0 ug/1 PAP 07/28/99 0812
< 5. 0 5 .0 ug/1 PAP 07/28/99 081.2
< 5. 0 5.0 ug/1 PAP 07/28/99 0812
< 5. 0 5.0 ug/1 PAP 07/28/99 0812
< 5 .0 5 .0 ug/1 PAP 07/28/99 0812
< 5.0 5 .0 ug/1 PAP 07/28/99 0812
10 .o 10.0 ug/1 PAP 07/28/99 0812
< 10 .0 10.0 ug/1 PAP 07/28/99 0812
< 5.0 5 .0 ug/1 PAP 07/28/99 0812
000065
Davis & Floyd, Inc. I PO Drawer 42U I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 2%49 I [phone] I Fax [phone]
DAYIS
FLtlYD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS
1.,1-DICHLOROETHENE
BENZENE
CHLOROBBNZENE
TOLUENE
TRTCHLOROETHENE
: LCS183BS:1
20 00
20 00
20 00
20.00
20.00
18.79
19. 47
18. 59
19 84
19.05
Report Date
Page 1 of 1
Augunt 11, 1999
Matrix GW/ChemW
WorkGroup: WG18385
Method
94.0
97.4
93.0
99.2
95.3
SW846 82608
74-125
90-119
89-116
87-120
86-.120
Q.-00066 ·; '
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 ! }31 (J°L Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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Df\VIS
FLMD LABORATORY ANALYSIS REPORT
LaboraJory Control Standards and DuplicaJes
LCS
1,1-DICHLOROETHENE
BENZENE
CHLOROBBNZENE
TOLUENE
TRICHLOROETHENE
LCS18386:l
20.00
20.00
20.00
20. 00
20.00
17.65
19.32
19.12
19.62
18.59
Report Date
Page 1 of 1
Augui;1t 11, 1999
Matrix GW/ChemW
WorkGroup: WG18386
Method
88.3
96.6
95.6
98.1
93.0
SW846 82608
74-125
90-119
89-116
87-120
86-120
000067
Davis & Floyd, Inc. I PO Drawer 428 ! Greenwood, SC 29648 I Bl 6}. Durst Avenue I Greenwood, SC 29649 I [phone] j Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MG/M.SD
1,1-DICHLOROETHBNB
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
1,1-DICHLOROETHENE
BENZENE
CJ-ILOROl38NZENI::
TOLUENE
TRICHLOROETHENE
MS99072310-10:18385
MSD99072310-10:18385
50.00
50.00
50.00
SO.DO
SO.OD
50.00
50.00
50.00
SO.OD
50.00
Report Date
Page 1 of 1
Auguot 13, 1999
Matrix GW/chemw
WorkGroup: WG18385
Method
< 0.00500 39.54
< 0.00500 42.59
< 0.00500 40.93
< 0.00500 41.64
< 0.00500 40.50
42.63
44. 87
42. 96
44.64
43 .13
85.3
89.7
85.9
89.3
86.3
Q00068
SW846 82608
79.1
85.2
81.9
83.3
81. 0
7.52
5.21
4.84
6.95
6.29
74-130
89-120
89-115
86-120
86-122
9
10
6
7
12
74-130
89-120
89-115
86-120
86-122
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2%48 J 816 E. Durst Avenue I Greenwood, SC 29649 I (8()4) 229-4413 I Fax [phone]
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FLtJ\1D LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENB
TRICHLOROETHENE
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
MS99072310-21:18386
MSD99072310-21:18386
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
Report Date
Page 1 of 1
August 13, 1999
Matrix GW/ChemW
WorkGroup: WG18386
Method
< 0.00500 41.78
0.0531 100.8
< 0.00500 46.67
< 0.00500 47.40
< 0.00500 45.91
42.09
100,6
46.72
46.83
45.S5
84.2
95.0
93.4
93.7
91.1
Q0006!J
SW846 82608
83.6
95.3
93 . 3
94.8
91. 8
0.739
0 .179
0.107
1.21
0.787
74-130
89-120
89-115
86-120
86-122
' 10
6
7
12
74-130
89-120
89-115
86-120
86-122
Davis & Floyd, lnc. I PO Drawer 428 I Greenwood, SC 2%48 I 816 E.'_Dursl Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLfrYD LABORATORY ANALYSIS REPORT
Surrogates % Recovery
L99072310-l 7 OJ-AUG-99 12 :22 75. 1
L99072310-18 03-AUG-99 13 : 00 71.4
L99072310-19 03-AUG-99 13 : 39 75 .8
L99072310-20 03-AUG-99 14 : 1 7 75. 9
L99072310-21 03-AUG-99 17 : 2 8 59.3
L99072310-21 03-AUG-99 14 :55 85. 5
LCS18399:1 03-AUG-99 11 :04 79. 9
MB18399:1 03-AUG-99 10 : 2 6 74 . 5
MB18399:1 03-AUG-99 10 :26 74 . 5
MS99072310-19 :18399 03-AUG-99 16 : 12 73 . 4
MSD99072310-19:18399 03-AUG-99 16: so 68.3
TBP 2,4,6-TRIBROMOPHENOL
PBP 2-FLUOROBI PHENYL
2FP 2 -FLUOROPHENOL
NBZ NITROBENZENE-DS
PHL PHENOL-OS
TPH TERPHENYL~D14
75.S
63 . 7
74 .0
74. 8
82.1
80 . 4
74 . 9
78.4
78.4
76.3
77.9
Report Date
Page 1 of
August 11, 1999
Matrix
Method
42.8
36.1
42 . 6
45.1
38 .7
45. 2
44.7
46 . 2
46 .2
43 .1
38. 5
GW/Chemw
SW846 8270
85 . 3 32 .8
73 .5 28 .6
88 .s 34 .o
91. 7 35.4
85 .7 33 . 0
107.2 35. 8
86.1 36.4
90.9 37.9
90 . 9 37.9
91. 4 33 . 8
90 .2 31 .8
79.3
77 .5
82 .4
81. 3
83 . 5
83 . 3
85.8
84.9
84 . 9
84.1
86 .1
000070
Davis & Floyd, Inc. ! PO Drawer 428 I Greenwood, SC 2%4B~ I 816 L Durst Avenue I Greenwood, SC 29649 I (Bh4) 229-441] I F.ix (864) 229-71 I ~l
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FLOYD
Method Blanks
Blank
Parameter
Semivolatile Organics
SW846 8270C
1,2,4-TRICHLOROBENZENE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DICHLOROPHENOL
2,4-DICHLOROPHENOL
2,4-0IMETHYLPHENOL
2,4-DIMETHYLPHENOL
2,4-DINITROPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-CHLOROPHENOL
2-METHYL-4,6-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
2-METHYLNAPHTHALENE
2-METHYLPHENOL
2-METHYLPHENOL
2-NITROANILINE
2-NITROPH8NOL
MB18399:1
2-NITROPHENOL
3,3'-DICHLOROBENZIDINE
3-NITROANILINE
4-BROMOPHENYL PHENYL ETHER
4-CHLOR0-3-METHYLPHENOL
4-CHLOR0-3 -METHYLPHENOL
4-CHLOROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-METHYLPHENOL
4-METHYLPHENOL
4-NITROANILINE
4-NITROPHENOI,
4-NTTROPHENOL
ACENAPHTHENE
LABORATORY ANALYSIS REPORT
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
Cone
10 . 0
10.0
10 .o
10.0
10 . o
10 .0
10.0
10.0
10.0
10 .o
10.0
10 .o
25 . 0
25 . 0
10.0
10. 0
10 .0
10.0
10 .0
25 .0
25 . 0
10 .o
10.0
10.0
10.0
10 . 0
10.0
10.0
10. 0
10. 0
10 .o
10 . 0
10.0
10.0
10. 0
10 .o
10 .0
25. 0
25. 0
10 . 0
0000'71
Report Date August
Page 1 of 3
Matrix GW/ChemW
WorkGroup: WG18399
Qual RDL Units
10 .0 ug/1
10.0 ug/1
10.0 ug/1
10 .0 ug/1
10 . 0 ug/1
10 .0 ug/1
10 . 0 ug/1
10.0 ug/1
10.0 ug/1
10.0 ug/1
10.0 ug/1
10.0 ug/1
25.0 ug/1
25. 0 ug/1
10 .o ug/1
10 .o ug/1
10.0 ug/1
10.0 ug/1
10.0 ug/1
25.0 ug/1
25.0 ug/1
10 . 0 ug/1
10.0 ug/1
10 .0 ug/1
10. 0 ug/1
10.0 ug/1
10 .0 ug/1
10.0 ug/1
10.0 ug/1
10.0 ug/1
10.0 ug/1
10.0 ug/1
10.0 ug/1
10.0 ug/1
10 .0 ug/1
10.0 ug/1
10.0 ug/1
25.0 ug/1
25. 0 ug/1
10.0 ug/1
11, 1999
Analyst Date Time
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/nsn 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1.026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1 026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
JRN/DSD 08/03/99 1026
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2%48 I Bl 6 L Durst Avenue I Greenwood, SC 29649 I (864) 229-44 lJ I Fax [phone]
DAYIS
FLtiYD
Method Blanks
Blank MB18399:1
Pou::ameter
ACENAPHTHYLENE
ANTHRACENE
BENZO(A)ANTHRACENE
BENZO(A)PYRENE
BENZO{B)FLUORANTHENE
BENZO(G,H,I)PERYLENE
BENZO (K) FI,UORANTHENE
BENZOIC ACID
BENZYL ALCOHOL
Bii>(2-CI-ILOROETHOXY)METHANE
BIS ( 2 -CHLOROETHYL) ETHER
BIS (2-CHLOROI.SOPRO!'YL) ETHER
BIS (2-ETHYLHEXYL) PHTHALATE
BUTYL BENZYL PHTIIALATE
CHRYSENE
DI-N-BUTYL PHTHALATE
01-N-OCTYL PHTHALATE
DIBENZ (A, H) ANTHRACENE
DIBENZOFURAN
DIETHYL PHTHALATE
DIMETHYL PHTHALATE
FLUORANTHENE
FLUORENE
HEXAC!lLOROBENZENE
IIEXACHLOROBOTADIENE
HEXACHLOROCYCLOPENTADIENE
HEXACHl,OROETHA.N'E
INDEN0(1,2,3-CD}PYRENE
ISOPHORONE
N-NITROSODI-N-PROPYLAMINE
N-NITROSODIPHENYLAMINE
NAPHTHALENE
NITROBENZENE
PENTACHLOROPHENOL
PENTACHLOROPIIENOL
PHENANTHRENE
PHENOL
PHENOL
PYRENB
SW846 8270(.' DOWTHERM
1, l' -Bl PHENYL
BIPHBNYL ETIIER
LABORATORY ANALYSIS REPORT
Report Date Augu~t 11, 19 99
Page 2 of
Matrix GW/ChemW
WorkGroup; WG18399
Cone Qual RDL Uni ta Analyst Date Time
< 10.0 10.0 ug/1 JRN/DSD 08/03/99 1026
< 10.0 10. 0 ug/1 JRN/DSD 08/03/99 1026
< 10.0 10 .o ug/1 JRN/DSD 08/03/99 1026
< 10 .o 10.0 ug/1 JRN/DSD 08/03/99 1026
< 10.0 10.0 ug/1 JRN/DSD 08/03/99 1026
< 10.0 10 . 0 ug/1 JRN/DSD OB/03/99 1026
< 10 .0 10.0 ug/1 JRN/DSD 08/03/99 1026
< 50.0 50 .0 ug/1 JRN/DSD 08/03/99 102 6
< 10. 0 10.0 ug/1 JRN/DSD 08/03/99 1026
< 10.0 10.0 ug/1 ,JRN/DSD 08/03/99 1026
< 10.0 10.0 ug/1 JRN/DSD 08/03/99 1026
< 10 . 0 10.0 ug/1 JRN/DSD 08/03/99 1026
< 10 .0 10.0 ug/1 JRN/DSD 08/03/99 1026
< 10.0 10 .o ug/1 JRN/DSD 08/03/99 1026
< 10 .0 10.0 ug/1 JRN/DSD 08/03/99 1026
< 10 .0 10.0 ug/1 JRN/DSD 08/03/99 1026
< 10.0 10 .0 ug/1 JRN/DSD 08/03/99 1026
< 10 .0 10. 0 ug/1 JRN/DSD 08/03/99 1026
< 10.0 10. 0 ug/1 JRN/DSD 08/03/99 1026
< 10 . 0 10.0 ug/1 JRN/DSD 08/03/99 1026
< 10.0 10.0 ug/1 JRN/DSD 08/03/99 1026
' 10 . 0 10 .0 ug/1 JRN/DSD 08/0J/99 102 6
< 10.0 10.0 ug/1 JRN/DSD 08/03/99 1026
< 10.0 10.0 ug/1 JRN/DSD 08/03/99 1026
' 10.0 10.0 ug/1 JRN/DSD 08/03/99 l 02 6
' 10.0 10.0 ug/1 JRN/DSD 08/03/99 1026
< 10. 10.0 ug/1 ,TRN/D.SD 08/03/99 1026
< 10.0 10.0 ug/1 JRN/DSD 08/03/99 1026
' 10 .0 10 .0 ug/1 JRN/DSD 08/03/99 1026
< 10.0 10 . 0 ug/1 JRN/DSD 08/03/99 1026
< 10 . 0 10 .o ug/1 JRN/DSD 08/03/99 1026
< 10.0 10.0 ug/1 JRN/DSD 08/03/99 1026
' 10.0 10. 0 ug/1 JRN/DSD 08/03/99 1026
< 25 . 0 25.0 ug/1 JRN/DSD 08/03/99 1026
< 25.0 25.0 ug/1 JRN/DSD 08/03/99 1026
' 10.0 10. 0 ug/1 JRN/DSD 08/03/99 1026
< 10.0 10.0 ug/1 JRN/DSD 08/03/99 1026
' 10.0 10 . 0 ug/1 JRN/DSD 08/03/99 1026
< 10.0 10.0 ug/1 JRN/DSD 08/03/99 1026
< 10.0 10.0 ug/1 DSD/JRN 08/06/99 0935
< 1 0 . 0 10.0 ug/1 DSD/JRN 08/06/99 0 93 5
00007~?
D;ivis & Floyd, !nc. I PO Drawer 428 I Greenwood, SC 29(,4H I 81 b E. Durst Avenue I Greenwood, SC 29fi4~J l (tlh4) 22~J-4413 I Fax (H64) 229-7119
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FLOYD
Method Blanks
Blank MB18399:l
Parameter
Analytical Prep Procedures:
ACID EXTRACTABLES SW846
BNA SEMIVOLATILES SW846
OOWTHHRM SW846
LABORATORY ANALYSIS REPORT
3500B
3500B
3500B
Report Date
Page 3 of 3
August 11, 1999
Matrix GW/ChemW
WorkGroup: WG18399
Cone Qual
JMT 07/27/99 0830
JMT 07/27/99 0830
JMT 07/27/99 0830
000073
RDL Units Analyst Date Time
Davis & r-loyd, Inc. I PO Drawer 42a I Greenwood, SC 29648 I 816 F.. Durst Avenue I Greenwood, SC 29649 I [phone] ! Fax [phone]
DA.YIS
FLt1YD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS LCS18399:1
1,2,4-TRICHLOROBENZENE so . 00
1,4-DICHLOROBENZENE 50 .00
2,4-DINITROTOLUENE so. 00
2-CHLOROPHENOL 75. 00
4 -CHLOR0-3-METHYLPHENOL 75. 00
4-NITROPHENOL 75 . 00
ACENAPHTHENE 50 .00
N-NITROSODI-N-PROPYLAMINE 50.00
PENTACHLOROPHENOL 75 . 00
PHENOL 75 .00
PYR8NE 50 .00
32 .46
33 .88
41 . 30
51 . 60
53 .19
17 .38
39.51
45.08
35. ••
27 . 50
39 . so
Report Date
Page 1 of 1
: Auguot 11, 1999
Matrix GW/ChemW
WorkGroup: WG18399
Method SW846 8270C
64 • 9 31-96
67.B 31-93
82 • 6 39-114
68.8 34-101
70.9 44-102
23 • 2 9-49
79 . 0 34-109
90 ., 36-107
47.B D-88
36 .7 15-49
79 .6 43-116
000074
O;ivis & r:loyd, Inc. I 1'0 Drawer 42H I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29(,49 I {864) 229-4413 I Fax [phone]
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FLOYD. LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
1,2,4-TRICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4-DINITROTOLUENE
2-CHLOROPHENOL
4-CHLOR0-3-METHYLPHENOL
4-NITROPHENOL
ACENAPHTHE:NE
N-NITROSODI-N-PROPYLAMINE
PENTACHLOROPHENOL
PHENOL
PYRENE
1,2,4-TRICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4-DINITROTOLUENE
2-CHLOROPHENOL
4-CHLOR0-3-METHYLPHENOL
4-NITROPHENOL
ACENAPHTHENE
N-NITROSODI-N-PROPYLAMINE
PENTACHLOROPHENOL
PHENOL
PYRENE
MS99072310-19:18399
MSD99072310-19:18399
50. 00
50 . 00
50 . 00
75. 00
75 .00
75. 00
50.00
50.00
75. 00
75 .00
50. 00
50. 00
50. 00
50. 00
75. 00
75.00
75.00
50.00
50.00
75.00
75.00
50.00
< 0 .0100
< 0 .0100
< 0 .0100
< 0 .0100
< 0.0100
< 0. 02 so
< 0.0100
< 0 .0100
< 0 . 0250
< 0 .0100
< 0 . 0100
32.26
35. 34
39.51
so. 41
47.80
11 . 65
41 .90
42 .17
16 . 72
24 . 48
39 . 80
Report Date
Page 1 of l
Auguot 11, 1999
Matrix GW/ChemW
WorkGroup: WG1B399
Method SW846 8270C
32.77 65.5 32-92
34. 98 70 . 0 2 9-92
40 .54 81 .1 37-1-15
51 .91 69 .2 35-97
50. 42 67 .2 44-102
15 . 07 20 . 4-71
41 .05 82 . l 4 0-104
44.24 88. 5 39-106
". 27 39 . 0 11-126
25 . 94 34. 6 4-70
39. B6 79 .7 43-112
" . 5 1.57 32 32-92
70. 7 1.02 35 29-92
79. 0 2.57 25 37-115
67.2 2.93 31 35-97
63 . 7 5.33 21 44-102
15 .5 25.6 27 4-71
83. 8 2 .05 26 40-104
" . 3 ' . 79 28 39-106
22 .3 54.6 28 11-126
32. 6 5 . 79 28 4-70
79 ., 0 . 151 19 43-112
000075
0;ivis & Floyd, Inc. I PO Drawer 428 \ Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLtwD
Method Blanks
Blank
Parameter
Gas Chromatography
SW846 8015
ETHYLENE GLYCOL
MB18431:1
LABORATORY ANALYSIS REPORT
<
Report Date
Page 1 of 1
Augu~t 11, 1999
Matrix GW/ChemW
WorkGroup: WG18431
Cone Qual RDL Units Analyst Date Time
7.0 7.0 mg/1 JAW OB/02/99 1138
000076
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29(,48 I 816 E. Durst Avenue I Greenwood, SC 2%49 I (864) 229-44 JJ I fax [phone]
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FLtwD LABORATORY ANALYSIS REPORT
Laborat01y Control Standards and Duplicates
LCS : LCS18431:1
ETHYLENE GLYCOL 50.00 47 .14
Report Date : Auguot 11, 1999
Page 1 of 1
Matrix GW/ChemW
WorkGroup: WG18431
Method SWB46 8015
94.3 64-117
000077
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue ! Greenwood, SC 29649 I [phone] I Fax {864) 229-7119
DA,YIS
FLOYD· LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
ETHYLENE GLYCOL
ETHYLENE GLYCOL
MS99072310-03:18431
MSD99072310-03:18431
50.00
50. 00
310.3
875.9
Report Date
Page 1 of 1
Augu~t 11, 1999
Matrix GW/ChemW
WorkGroup: WG18431
Method SW846 8015
837.5 105.4 73-116
113 .1 4.48 20 73-116
000078
Davis & Floyd, Inc. I PO Drawer 42B I Greenwood, SC 29648 J 816 E. Durst Avenue j Greenwood, SC 29649 I [phone] I Fax [phone]
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FLtwD
Parameter
Wet Chemistry
SW846 9060
Method Blanks
Blank MB18389:l
ORGANIC CARBON, TOTAL
LABORATORY ANALYSIS REPORT
Report Date Augu~t 11, 1999
Page 1 of 1
Matrix GW/ChemW
WorkGroup: WG18389
Cone Qual RDL Units Analyat Date Time
< 1.0 1. 0 mg/1 TRB 07/26/99 1502
000079
Davis & Floyd, Inc. I PO Drawer 42B I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLt1YD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
Report Date : Augu□t 11, 1999
Page 1 of 1
Matrix : GW/ChemW
LCS LCS18389:1 WorkGroup: WG18389
Method SW846 9060
ORGANIC CARBON, TOTAL 10.00 10. 30 103.0 90-110
000080
Davis & Floyd, Inc. / PO Drawer 428 I Greenwood, SC 29648 I 816 I:. Durst Avenue I Greenwood, SC 2%49 j (8fi4) 229-4413 I rax [phone]
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FLifYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
ORGANIC CARBON, TOTAL
:,:,·, /:·:: .'',,,_
'}:J:ra~~;e~
ORGANIC CARBON, TOTAL
MS99072310-14:18389
MSD99072310-14:18389
Report Date
Page 1 of 1
Matrix
Auguot 11, 1999
GW/ChemW
WorkGroup: WG1B389
Method SW846 9060
4.38 26.90 112. 6 77-121
000081
Davis & Floyd, Inc. j PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29(>49 I (ll64) 229-4413 I Fax [phone]
0
0
0
0 co
,'"\)
D~IS h(i,"'•1
.lniiledln FL YD 1mr..-.i ,~ !mi"'
Client Project I Site LocatJon
Ticona 60885.00,
Shelby,NC
Contact Report To
Jeff Randolph
Collected By
J.G. Jenldns, Ill
NOTICE:
Sample Collection
Sample Descrintion Date Time
T~i'n Rl-_1, 1/2,/qq I\~ ... "
fiU~7, r 17.0O
J./U-H'o /70(.,
1'. Tr. .I /7Xn
r . LJ q I I-/ I q
T· ,.S /. r z.ro
FE. · 5 9, 11, I I
FF·3L-\ 11//,
Ff,{,?.., l,7.,
(j..f:. (, I 1 /, ?'4' /0(7
AA-C:'-1 10.59,
v-s/1, 110<
I 11:' r::: )13.0
1 iE" F /7"t.n
k--z.9, /_"',7c)
Reliquishe , L .,ljlfl Time Reliquished By
tni. ' rli' (\'if ?..t)
rreceived B . uate Time Received By
vomments
Matrix Type Definitions 1 -Drinking Water 2 -Clean Water 5 -Groundwater
Chain of Custody Record Page --of_]___
816 E. Durst Avenue, Greenwood, SC 29649 [phone] Fax: [phone] Ce vse vn,y
Laboratory Certifcation Numbers: SC· 24110, NC-25, TN· 2923, VA· 77
Copy To Reporting Requirements: [ J Standard { } Data Package (Specify Leval) urchase Order
Required Parameters, Containers end PreseNativas State Quote ~-"' "' " ;i NC E E. E fr ~ ~ E e; N -0 ~l L0!,.ll0 Special Instructions -. N •
" e :; j "' "8 I 0 0 ~~ ] ~ ;; ;, N • 0 •
8 "' :, C " C " ~ . 0 0 . ~~ " i3 ;; • C '> ~ 0 ~ '6 " E ~ • • • ii • :, ~ 0 0 X
C . ~" • il" ~ ~ t E ~ 5 E " " ·e :e 1 ~ !-?. 8 is • a e ;; i; :, z w ~~ ..J
Time Type Total B A C A Fraction HOT .... ommems
X .5 7.-?.-IJ.IJ.
>( t;, 2-., 01
')( C 7 7 07.,
x <; I 7 7 03
y 5 7..... L.. of/,,
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X c:; I 7..-, "Z.. ,3
X c:. -,, 1 ? //JI
Date Time Reliquished By Date Time Quick~ Shippr;;;J
y N ,.. CLIENT
"" ~EDEX
Date Time :;:~;n;'_"~: v/s
Date Time lfY,Jecify: Airbi/1 Number
7.H.00 01no __ days
CooleclD~ablo), /
On Ice: es I o Temp(C) J./.,
Custody Seal: Intact / Brok~n~
7 -Soil/Sediment 8 -Liquid Sludge 9-0il 12 -Air Davis & r-rcrya, Inc_ ---- ----__ .,_
----- - ----- -- -- - ---
0
0
0
0
00 w
Chain of Custody Record
Client Project I Site Location 816 E. Durst Avenue, Greenwood, SC 29649 [phone] Fax: {864) 229-7119
Tlcona 60885.00, Laboratory Certifcation Numbers: SC-24110, NC-25, TN-2923, VA· 77
Shelby,NC
Contact Report To Copy To Reporting Requirements: { J Standard { } Data Package (Specify Level)
Jeff Randolph
Collected By Required Parameters, Containers and PreseNatives
=g " " g < li ! ~! c\ J.G. Jenkins, Ill ~} N •• •
NOTICE: u • s "' 1l 2 • iil § 5 it N • C 8 "' " "8 0 . '-' ... 5 ~ ~-s 15 " • E ~ ·;;; • • " • ; ~ 0 C ]u ~ Jl ~ • .-:; -~ ~ E '-' ,. "ER Sample Collection -1l. -~ .,: , 0 c\\ \2 J; £:! z
Samote Descriotion Date Time Time Type Total B A C A
l/. 7 .... 1/nh, I ,r~ y ,\ "2 , ?
l'l'-<3 I,_, ,:, )( t::., 7 -z...
p F IA,. 1-/ 1.,1< 'l( r:; 7, 1 ,
7c;,.,_j.j f) • -, } : ,' . l ~ 151,;-x c::: ' -z_ I . . PE u 1 • 3 I h ?J.l )( c; C, "2... ~
Df111-/ 16,<:" I Y ,; <. 1... I
r:-<;(i ,, /J./ 'I -<, 2.... /
Rrquished By. L Date Time Reliquished By Date Time Reliquished By Date Time
' , li.,/q, 0 8,'7./'J I 'I'\ '" -'\l"eived ' 'Date Time Received By Date Time TJ;;L'i;;775o r;.s
Date Time
7-J. ~.,:ii.) O.fJO
..,ommenis
Matrix Type Definitions 1 -Drinking Water 2 -Clean Water 5 • Groundwater 7 -Soil/Sediment 8 -Liquid Sludge 9-0il 12 -Air
Preservative Definitions A -None B • H2S04 C -HCI O • HN03 E -NaOH F • Filtered G -Oltler
Page _L of ..1..._
,....,,,ce use umy
urr:hase Order
Stare Quote
NC
Login Special Instructions
I<) a
i~ j g ~ ~ . ~; •• ~i i ~ _,
Fraction HOT omments
/5
/le
17-
/8
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Quick TAT Shic:;Jy y0 CLIENT
"" FEDEX
If Y, specify: Airbill Number
__L days
Coole"D ~able), /
Oo tee, e, I o Tomp(C)
0
b
Custody Seel: Intact / Broken Non
Davis & r-1oyo, Inc.
FL02_01 (02199)
Di\)/1S
FLOYD
(HGlN(CRS ARCHITECTS
PLANNCRS SCIENTISTS
FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS CHARLESTON • GREENWOOD • COLUMBIA Well No · H 14-q 1 ..
Client: J,"e,ang Source(,) of Well IO Mer 10 Label ~no)
Sile Name: S1,\b,11 ll-c. Job No.: ii 0th:5. o o Well Completion: Protective Cosing ~o) Flush {yes'Q
Dale: 7-Ll-~q LWR submilled by: -Flush-I.fount Cover Seal lnlacl (yes/no) Lacking Cap {yes/no)
Sampling Personnel: -:r.&. :;r,. oki',r m Lacked of Arrival @,a) Departure (G;Jno)
Si1e Personnel: -Well Casing {heigh! obove/deplh below) ground: z., fl.
Regulatory Personnel: -Casing Type (PVC) {~ {Other)
Weather Conditions: lle«r Temp.: ~v Dedicated~ or Bailer €Jna) Type
Well Oiameler: l,_ 0 In. Proleclive Post/ Abutment {yes~ Concrete Pod @no)
(A) Top af Well [levalion: 755.07 ms! {yes/no) Well Integrity Satisfaclory0n~;"' explain below.
(B) Oeplh lo Immiscible Layer. N/ttt. Well Yield ( law / maderofe / high
(C) Immiscible Layer [levalion: (A)-(B)= /:;L d ms! (yes/no)
(0) Oepfh lo Groundwater. iio.;:i1 II. W[LL VOLUl.f[ DATA
([) Groundwater [levation: (A)-(0)= l/S • .Sb msl (yes/no) DIA. or PIPE (In.) VOLUME IN GAL/rt.
1.0 0.041
(r) Total Well Depth = 11 ff. 2.0 0.163
' 3.0 0.367
(G) Length of Waler Column: (F)-(D)= "!:, h-h 'l f I. 4.0 0.653
~ 5.0 1.020
Casing Volume = {G) x Volume in gol./11.= gals. 6.0 1.470
Method of Well [vacuotion PvmGl S1qrf Time: Ill C TO CONVERT GAL/rT TO LITERS/rT, MULTIPLY ABOVE FIGURES BY
Method of Sample Collection fv "1@ I loo 3.8 LITERS/GALLON.
Time:
Chain-of-Custody Form Started 0s}no)
FIELD ANALYSES
Isl Volume 2nd Volume 3rd Volume 4th Volume 5th Volume
Volume. Purged (gallons) l I ,, I 7/.l ~'{/
Time {mililary) IIW /1?..S-I~~ 1/S-'L / : ()0
pH (S.U.) '7 <;-' 7.:..., " I,. -r. .s-
Sp. Cond. {umhos/cm) .fL 'I. r I 'i q "\ ,, 7
Waler Temp. (•c) lo-,r / 2 I 0 ,,
Odor {subjective)• . I I I I
Turbidity (subjective)" . i I I I I
• (l)None (2)Slighl (3)Moderole {4)Slrong
" (1)Clcar (2)Slighlly Turbid (3)Moderolely Turbid (◄)Very furbid (S)Exlremely Turbid
Commcnls/Observolions/Recommendalions: _:rn=~l~i::~o=,l>O=.ulh'-C.ju/LLI -------------------
fORM COMPLETED BY:
DATE:
O& r form48 (3/94)
000084
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FLttfD
ENGINEERS
PLANNERS
ARCHITECTS
SCIENTISTS
FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
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CHARLESTON • GREENWOOD • COLUMBIA
Well No · HI/ · J.j S ..
Clienl: L'a.1ng Source(,) of Well ID t'l0f ID Lobel 8-no)
Site Nome: S 11,lb,,1 f::JC. Job No.: ti Or:fl:5. 0 0 Well Completion: Proleclive Cosing ©no) flush (yes&
Dafe: 7·7,/-~q LWR submilled by: -flush-Moun! Cover Seal Intact (yes/no) Locking Ccp (yes/no)
Sampling Personnel: 'T, C,. -:r ~ ok,·., ' [fJ_ Locked of Arrival ~o) Deporlure (€i}J,o)
Sifo Personnel: -Well Cosing (height above/depth below) ground: 1-S" II
Regulolory Per>onnel: -Cosing Type (;VC) (~ {Other)
Weather Conditions: l 1~6c Temp.: 'ir:,\ Dedicoled ~ or Boiler <i2:'no) Type ·
Well Oiomeler: 1 .. 0 In. Prolective Posi/Abulmenl (yeskY Concrete Pad ~no)
(A) Top of Well Elevolion: 755 · 1:1':I msl (yes/no) Well lnlegrily Solisf~~ {.).)no) If no, explain below.
(B) Deplh to Immiscible Loyer. Nftn. Well Yield ( low / od;,~ high )
(C) Immiscible Layer Elevalion: (A)-(B)= f,,l d msl (yes/no) -
(D) Depth to Groundwater. ~0.30 II. WELL VOLUME DATA
(E) Groundwoler Elevalion: (A)-(D)= 7 t.t. H':l msl (yes/no) DIA. or PIP[ (In.) VOLUME IN GAL/ft.
1.0 0.041
(f) Tofal Well Deplh = H~ ft. 2.0 0.163
(G) Lenglh of Waler Column: (F)-(0)= J.-, fl. 3.0 0.367
4.0 0.653
/, 3 5.0 1.020 Casing Volume = {G) x Volume in gal./ft.= gals. 6.0 1.470
Method of Well Evacuation 5a.!•fl Stqrt Time: /Qso TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOVE flGURES BY
p,,,n/1 \1 l!l\2 3.8 LITERS/GALLON.
Method of Sample Collection Time:
Chain-of-Custody form Slorled /i ye,s/no)
FIELD ANALYSES Sq .. ~IG. . 1st Volume 2nd Volume 3rd Volume 4th Volume 5th ••'"fllume
Volume Purged (gallons) '· i ?_,(.(·rn\ ~
nme (military) 105"1', ,, ,,.,, ~ ,-,;;, .
pH (S.U.) "i . ..., " . .., -( q
Sp. Cand. (umhos/ cm) I,,.,_ , ... ,_ 7.
Waler Temp. ("C) , I q jq
Odor (subjective)• I I I
Turbidity (subjective)" . I I ' • (1)None (2)Slighl (3)Moderole (4)Slrang
" (l)Clear (2)Slighlly Turbid (3)Moderalely Turbid (4)Very forbid {S)Exlremely Turbid
Commenls/Observations/Recommendolions: _T.,_.,R,l,,(L, -=-~_,o,..,."'-cx,"'-'~!!>,~~' 1-! -------------------
FORM COMPLETED BY: 8;) w , 17P
OAT[: _ i~~ _
O& r form48 (3/94)
000085
CNCINEERS ARCHITECTS FIELD DAT A LOG D1')/1S
FLOYD PLANNERS SCIENTISTS
CHARLESTON • GREENWOOD • COLUMBIA
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
Clienl: TilOf\Q
Sile Nome: S)i,\b,,1
Dole: 7 -L / · q q
Job No.: 6 OtfrS. o o
LWR submilled by: ______ _
Sampling Personnel: _°T.:,_c•_,,&'-'.~-'A>LLl".LDu,/(._,,'""•(..,, _.,_JEi.;-___ _
Site Personnel: ___ -____________ _
Regulolory Personnel: ______________ _
-----~--_ms! {yes/no)
N/tll.
{C) Immiscible Loyer [lcvo n: {A)-{B)= A/ A ms! (yes/no)
{D) Dcplh to Groundwoler. . _,_ __________ _:_:.:II.
______ ms! {yes/no)
{F) Toto! Well Depth = ----->.----------=ti.
{G) Length of Wolcr Column: (F)-{D)= ___________ t_l.
Cosing Volume = (G) x Volume in goi./fl. , ______ _,_,o=ls.
Method of Well Evacuation ______ l~rl Time: ___ _
Method of Sample Collection---:= ____ Time: I 7 S: ()
Chain-of-Custody form Started
Well No.: T. Tl J;...
Mep ID Lobel (yes/no)
Well Com elion: Proleclive Cosing (yes/no) flush {yes/no)
ver Scot Intact {yes/no) Locking Cop (yes/no)
Locked al Arrival es/no) Deporlure {yes/no)
Well Cosing {heigh! o ve/dcplh below) ground: _____ ..1f1,_I.
Cosing Type {PVC) {Steel Olher) __________ _
Dedicated Pump or Boiler ( s/no) Type
Protective Post/ Abulmenl {yes/ no Concrele Pad {yes/no)
Well Integrity Solisfoctory {yes/no) If o, explain below.
Well Yield ( low / moderale / high )
WELL VOLUME DATA
DIA. or PIPE (in.) VOLUME IN GAL/Ft.
1.0
2.0
3.0
4.0
5.0
6.0
0.041
0.163
0.367
0.653
1.020
1.470
TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOVE flGURES BY
3.6 LITERS/GALLON.
FIELD ANALYSES
Volume Purged (gollonsf
Time (military)
pH (S.U.)
Sp. Cond. (umhos/cm)
Water Temp. ("C)
Odor (subjective)•
Turbidity (subjeclive)"
1st Volume
-
• (l)None (2)Slight (3)Moderale (4)Slrong
2nd Volume 3rd Volume
" {l)Cteor (2)Slighlly Turbid (3)Moderalely Turbid (4)Very forbid (5)Exlremely Turbid
4th Volume 5th Volume
~
I ?,«-tJ -' .,_
L c.--u
I 4-
'
Commenls/Observalions/Recommendolions: _1,.,R,"'-'-{.'-';'-..,l'Jc..c·.,.OO="'.,u¥-/ _,_) __________________ _
FORM COMPLETED BY: ~~:~~l: 11Ef
DATE: L7-/L~ ~
D& r form4B (3/94)
000086
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I D~S ENGINEERS ARCHITECTS FIELD DATA LOG
FL D PLANNERS SCIEN TIS rs FOR GROUNDWATER SAMPLE COLLECTION/
CHARLESTON• GREENWOOD. COLUMBIA GROUNDWATER ELEVATION MEASUREMENTS ,, O
1·.------.---------~.---'---------~W~el~l~No~.:~C~~=-=~=1=...,
I
Client: T1°lOnq Source(,) of Well ID M0f ID lobel~no)
Sile Name: She\b,,1 f\}. C. Job No.:6Ot!r5. 00 Well Completion: Protective Cosing (!j'no) flush (yes~
Dale: 7· L/ -q q LWR submitted by: __ -_____ flush-Mount Cover Seal Intact (yes/no) locking Cap (yes/no)
Site Personnel: -Well Casing (height above/depth below) ground: J-1, $" fl. I Sampling Perso-n-ne_l= __ ::r_. &_. _::r_~_o_/_<_,••_' __ l[!_.____ Locked at Arnval@,no) Departure (&no)
Casing Type~) (Steel) {Other) __________ _
Dedicated ~or Bailer @/no) Type
Regulatory Personnel:_=-::...,.. ___________ _ I Weather Condilions: __ .=C:....ulc.,,~._ _____ Temp.: 9 0
Well Oiameler:. ______ 'Z...=·-()=-__ tn.
I ~:: :::,:r10w::::::~~::n~a-y-er.~. =..,-S "'-h~tf~~-:!N:'=/t==fl-. _msl (yes/no)
(C) Immiscible layer [levafion: (A)-(B)=......,A.,_/..,_A.,___ msl (yes/no) I (D) Depth ta Groundwoler.. ____ ,_/=B~-,~3 ... B.,_ ___ ~ff.
(£) Groundwater Elevation: (A)-(D)= n':J 5, J 3 msl (yes/no) I (F) Tolol Well Depth= -------~~q.,__ ___ ~ff.
(G) Length or Waler Column: (F)-(D)= --~3>~0=. _.,(,L'L-= __ r_t. I Casing Volume = (G) x Volume in gol./ft.= ___ ~5~-~g_ol~•·
Method of Well [vacuafion Pu mGJ Start Time: I '!,'i)
I Method of Sample Collecfion P~ Time: ./ ~ I q
Chain-of-Cusfody Form Started~no)
Protective Posl/Abulmenl Q;},no) Concrete Pod@no)
Well Integrity Salislaclory@~o, explain below.
Well Yield ( low / moderole ~
W[LL VOLUME DATA
DIA. OF PIPE (in.) VOLUME IN GAL/rt.
1.0
2.0
3.0
4.0
5.0
6.0
0.041
0.163
0.367
0.653
1.020
1.470
TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOVE flGURES BY
3.8 LITERS/GALLON.
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FIELD ANALYSES
tsf Volume 2nd Volume 3rd Volume 4th Volumo 5th Volume
Volume Purged (gallons) (: JO
Time (military) I ,,s-s-lt.\Ob IH 1,
pH (S.U.) c,. I .~,/ F,. 1
Sp. Cond. (umhos/ cm) '2.-Z. (, 7
Waler Temp. ("C) I q / i I 4
Odor (subjecfive)• I ' I
Turbidity (subjective)" -I ' I
• (!)None (2)Slight (3)Moderale (4)Slrong I .__•_•_(~1'-)C_te_o_r -'-(2.c.)s_r.c.1g_hl-'-ly_T_u_rb_id_(c...3.c..)M_o_de_r_at_el~y,:,T-,urb_id-'(-'4)~v_ery.,_r_ur,brcid,-,(-'5)~E_xl_re_m_e.c.ly_T_urb_id _______________ ~
Comments/Observofions/Recommendofions: 'T f<_ C::. /:). r:i) .,., / / I ~~v -------
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roRM COMPLETED BY: ~-B-&i!' flP
OAT[: J_ fi_~
O& r formiB (3/94)
000087
CNCINEERS ARCHITECTS FIELD DAT A LOG Di\}11S
FLOYD PLANNERS SCIENTISTS
CHARLESTON • GREENWOOD • COLUJ.(81A
FOR GROUNDW A TEA SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
Well No · T· S ', .. ,_
Client: L·iang Source(s) of Well ID t'\q\2 ID Label ~no)
Sile Name: S)i,\b,,1 t-J c. Job No.: 6, 0'!::fi:5. 0 0 Well Completion: Prolecfive Casing ~no) flush (ycse
Dale: 7· ZJ-~q LWR submilled by: -flush-t.founl Cover Seal lnlacl (yes/no) Locking Cop (yes/ no)
Sampling Personnel: J:. C,. :r,.ok,·.1 ' lJJ Locked of Arrival g:)/no) Departure 9'0)
Sile Personnel: -Well Cosing (heigh! obovo/deplh below) ground:
Regulatory Personnel: -Casing Type (PVC) @ (Other)
Weather Conditions: CI eqr T emp.:9 C{(ff,, Dedicated !'.!!!!)p or Bailer @jl/no) Type ·
Well Diameter: (.,. 0 In. Proleclive Post/Abulmenl (yes/@ Concrete Pad &no)
(A) Top of Well Elevation: 121. is msl (yes/no) WeU Integrity Solisfodory ~o) If no, explain below.
(Bf Depth fa Immiscible Layer. NA-11. Well Yield ( low / fi~/ high )
(C) Immiscible Layer Efevafian: (A)-(B)= b.l8 msl (yes/no)
(D) Depth fa Groundwater. . 11 • 6 ] fl. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(D)= 765,J I msl (yes/no) DIA. or PIPE (in.) VOLUME IN GAL/Fl.
1.0 0.041
(F) Total Well Depth = 35./ f I. 2.0 0.163
3.0 0.367 (G) Length of Waler Column: (F)-(D)= 1~-0 ~ ff. 4.0 0.653
3 , '\ nnls.
5.0 1.020 Casing Volume = (G) x Volume in gal./fl.= 6.0 1.470
Method of Well Evacuation Pii~ Start Time: ~ TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOVE flGURES BY
Method of Sample Collection fvm~ .I.B LITERS/GALLON.
Time: IJ:2 I.,
Chain-of-Cusfady Farm Slarfed ((yes~no)
'
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 5th Volume
Volume Purged (gallons) 7,,. ~ 7.t 1/. i
Time (military) I 'f L I,. ,TOI I riiJ
pH (S.U.) . 5. I 5,r,, <;. I. -
Sp. Cand. (umhos/cm) 1-l p,' so, 1>1.?
Wafer Temp. (•c) / '1 I 'I Jq
Odor (subjective)• I L 7
Turbidily (subjective)" " I l I
• (t)Nane (2)Slighf (3)Maderale ( 4)Slrong
" (1 )Clear (2)Slighfly Turbid (3)Moderolely Turbid (4)Very furbid (5)Exfremely Turbid
Commenls/Observafions/Recommendalions: _J.,_,,,R,,.C~-"'::_.,O'-'."o""o""-'"\.,._-0r-1l-1l'-----------------~
FORM COMPLETED BY:
DATE:
D& r form48 (3/94)
000()8~
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1D1\YIS
FLOYD
ENGINEERS
PLANNERS
ARCHITECTS
SCIENTISTS FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
••
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CHARLESTON • GREENWOOD • COLUMBIA
Well No · £ E -S 9:, ..
Clienf: L'c,,12og Source{,) of Well 10 Mep ID Label Q./no)
Sile Name: S)ielb,,1 f\}. c. Job No.: 6 O,:!s-.S. 0 0 Well Completion: Proledive Casing fi!jo) flush {yes/~
Dale: 7·Ll·9q LWR submilled by: -rlush-Mounl Cover Seal Intact (yes/no) Lacking Cap {yes/no)
Sampling Personnel: "T-&. :r ~ok,·•r . OJ. Locked al Arrival Gno) Oeparlure Q/no)
Site Personnel: -Well Casing {height above/depth below) ground: '2... ff,
Regulatory Personnel: -Casing Type {PVC) {Steel) (Other)
Weather Conditions: Pk±l:i Gb"I~ Temp.: 99 Dedicated Pump or Bailer Qno) Type
Well Diameter: 7..,, 0 In. Protective ~bulmenl (yes/Q) Concrete Pad ~o)
(A) Top of Well Elevation: 7 j~./.{"fi msl (yes/no) Well Integrity Satisfactory @~, explain below.
{BY Depth lo Immiscible Loyer. N/ttf. Well Yield ( low / moderale / hig
{C) Immiscible Layer Elevation: (A)-(B)= l::,l d msl {yes/no)
(0) Depth lo Groundwoler. . 2/;./!:j ff. WELL VOLUME DATA
([) Groundwater [levalion: (A)-(0)= 75&-2!-f msl (yes/no) DIA. or PIPE (In.) VOLUME IN GAL/rt.
1.0 0.041
(r) Total Well Deplh = S~-o f I. 2.0 0.163
7..,j,£(:, 3.0 0.367 (G) Length of Waler Column: (r)-(D)= fl. 4.0 0.653
~. 7 5.0 1.020 Casing Volume = {G) x Volume in gol./tt.= gals. 6,0 1.470
Method of Well Evacuation P11~ Starl Time: I Iit1 TO CONVERT GAL/rT TO LITERS/rT, MULTIPLY ABOVE rlGURES BY ~.,~ I b ti 3.8 LITERS/GALLON.
Method of Sample Collection Time:
Chain-of-Custody form Starled {tr:f no)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 5th Volume
Volume Purged (gallons) ), -, 7, l/ In, 7
Time (military} I ~-,C> I . <"" 1 11 /J 9
pH (S.U.) ,.1 h. 7 i .. 1 -
Sp. Cond. (umhos/ cm) II 0 ' L ~ I
Waler Temp. (•c) I 1 , , 7
Odor {subjective)• I I • I
Turbidity {subjective)" -I ', I .
• {1)None {2)Slighl {3)Moderafe (4)Slrong
" {!)Clear {2)Slighlly Turbid {3)Moderalely Turbid {~)Very forbid {5)Extremely Turbid
Commenls/Observalions/Recommendalions: _\~Q=(__=~Q~-~00~"6-['-I)~------------------
rDRM COMPLETED BY:
DAT[:
O& r form48 (3/94}
000089
Df\J/1S
FLtn'D
CNCINCERS ARCHITECTS
PlANHERS SCIENflSTS FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS CHARLESTON • GREENWOOD • COLUMBIA
Well No· FF-s~ .. -
Client: I,"c.ang Source(s) of Well ID Ma,., ID Lobel ~no)
Sile Name: Sh,\b,11 ~1-c. Job No.: lz 0tf1:5. 0 O Well Complelion: Proleclive Ca~ing ~no} flush (yo,,@)
Dole: 7·7,/·9q LWR submilled by: -Flush-Mounl Cover Seal Intact (yes/no) Lacking Cap (yes/no)
Sampling Personnel: "}".C,. -rt: ok,·•( lJ!. Locked of Arrival {;Jj,no) Oeparlure €J,io)
Siie Personnel: -Well Cosing (height above/depth below) ground: "L fJ.
Regulatory Personnel: -Casing Type (PVC) ~ (other)
Weather Conditions: ead-b lh11l~ Temp.: '.'I~ Dedicated Jum£_ or Bailer ~no) Type ·
Well Oiameler: 1,,0 In. Protective Post/Abutment (yes~ Concrete Pad {J;/no)
(A) Top of Well [levalion: 771-,3:; msl (yes/no) Well lnlegri~[actory ~no) If no, explain below.
(B) Depth lo Immiscible layer: N/tn. Well Yield low / moderate / high )
(C) Immiscible Layer £1evalion: (A)-(B)= !Jl d msl (yes/no)
(D) Depth lo Groundwoler: . 11-11 f I. WELL VOLUME DATA
([) Groundwater [levalion: (A)-(D)= 761, I b msl (yes/no) DIA. or PIPE (In.) VOLUME IN GAL/Fl.
1.0 0.041 (r) Total Well Depth = 3~.)(:) f I. 2.0 0.163
3.0 0.367 (G) length of Waler Column: (r)-(D)= L3-~3 f I. 4.0 0.653
1, t 5.0 1.020 Casing Volume = (G) x Volume in gol./fl.= gals. 6.0 1.470
Method of Well Evacuation ~lllll@ Stqrf Time: I bU: TO CONV[RT GAL/rT TO LITERS/rT, MULTIPLY ABOVE flGURES BY
(i),, mO l ]l c, 3.8 LITERS/GALLON. Method of Sample Collection Time:
Chain-of-Cusfody form Storied :.;;, (ye no)
FIELD ANALYSES 5~.,,~£J~~ 1st Volume 2nd Volume 3rd Volume 4th Volume
Volume Purged (gallons) ,. °' T.D /J (, ,i;; -Time (mililary) I .., "".? ,,,,, ,,TT
pH (S.U.) • L t, . {, -'~ . I, Sp. Cond. (umhos/cm) c;1· s-~ s-CJ
Water Temp. (•c) I 'b I ij 1r
Odor (s_ubiective)• ! I
Turbidity (subieclive)" . ~ '
• (l)None (2)Slight (3)Moderole (4)Slrong '
" (l)Cleor (2)Slighlly Turbid (3)Moderalely Turbid (4)Very forbid (5)Extremely Turbid
Comments/Observalions/Recommendalions: _J:...,R~l~=--~12-·~08(}~,..,~\-'-/ _,._/ _________________ _
FORM COMPLETED BY:
DATE:
D& r rorm48 (3/9•)
000090
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Di\}/1S
IFLtrl'D
[NCI NEE RS
PLANNERS
ARCHITECTS
SCIENJISTS
FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
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RLESTOH • GREENWOOD • COLUMBIA Well No· ff-6 L ..
Client: L·c.aog Source(,) of Well ID t:!0r1 10 Lobel ~no}
Sile Name: S11,\b,,1 f:J c. Job No.: k Oih:.S. 0 0 Well Complelion: Protective Cosing @o) flush (yes€1)
Dote: 7· L/-~q LWR submitted by: -flush-Mounf Cover Seal lnfocl (yes/no) Locking Cop (yes/no)
Sampling Personnel: "}'.(,. :r ~ok,·•r lJJ. Locked ol Arrival@' no) Oeparfure @no)
Site Personnel: -Well Cosing (heighl obove/deplh below) ground: 7-!I,
Regulatory Personnel: -Cosing Type (PVC) _(~ (Other)
Weather Conditions: e~i-1~ ~l,.,J~ Temp.: 'lS-Dedicated Pump or Bailer ®no) Type
Well Diameter: '} .0 In. Prolecfive ~Abutment (yes@ Concrele Pod (@no}
(A) Top of Well [levolion: 777,,,/" msl (yes/no) Well lnlegrily ~clory @no} If no, exploin below.
(Bf Depth to Immiscible Loyer. AJA-ft. Well Yield j low moderate / high )
(C) Immiscible Loyer [levolion: (A)-(B)= f,,l~ msl (yes/no) '
(D) Depth to Groundwoler. l/,4S f I. WELL VOLUME DATA
([) Groundwater Elevation: (A)-(D)= 760,11 msl (yes/no) DIA. or PIP[ (in.) VOLUME IN GAL/rt.
1.0 0.041
(F) Total Well Depfh = ~ 1,.. J.-1 0 ft. 2.0 0.163
50. q 1....-3.0 0.367 (G) Length of Waler Column: (F)-(D)= ft. 4.0 0.653
r£.3 5.0 1.020 Cosing Volume = (G)" x Volume in gol./ft.= gals. 6.0 1.470
Method of Well [vocuafion ~u~ Start Time: I~"" TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOVE FIGURES BY
~v•"° Time: /77 f'° 3.8 LITERS/GALLON. Method of Sample Colleclion
Chain-of-Custody Form Started ,. ';/~ (yes/n
FIELD ANALYSES 5 q"lf le
1st Volume 2nd Volume 3rd Volume 4th Volume 5th Volume
Volume Purged (gallons) f . ..._ j'/1/) I. ,11 12-~ -,--
Time (military) t707 I -,-I 7., s
pH (S.U.) ,. s " -l... /j
Sp. Cond. (umhos/ cm) 7 ( 7 ,...,~
Water Temp. (•c) 1 ~ . I ' I l',
Odor (subjeclive)• ' ' I Turbidity (subjeclive)" -I I I
• (!)None (2)Slighl (3)Moderale (4)Slrong
" (l)Cleor (2)Slighlly Turbid (3)Moderolely Turbid (4)Very forbid (5)Extremely Turbid
Comments/Observations/Recommendations: _T..u,R..,,l<..:.."-<0"--.'-'0"'01L.1ro"l~l\-,I-/ -1-J _________________ _
FORM COMPLETED BY:
OAT[:
0& r rorm48 (3/94)
000091
Df\YIS
FLOYD
[NCI NEE RS ARCUITECTS
PLANN[RS SCIENTISTS FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS CHARLESTON • GREENWOOD • COLUMBIA
Well No·{,_~-6 / ..
Client: J,""ang Source(s) of Well ID t10r . ID Label (i;}fno)
Sile Name: S"li,lb,,1 tJ c. Job No.: fr_ 0~Ji:5. 0 0 Well Completion: Protective Cosing~no) flush (yes9
Dale: 7· i1.-~q LWR submifled by: -flush-Mounl Cover Seal lnfocl (yes/no) Locking Cap (yes/ no)
Sampling Personnel: "}".C,. "J t: ok,'•( lJ!. locked af Arrival (i}o) Oeparlurc Wno)
Sile Personnel: -Well Casing (~e/depfh below) ground: "2-S-fl.
Regulatory Personnel: -Casing Type (PVC) @) (Ofher)
Weather Conditions: (, I 11, Temp.: (:0 Dedicaled Pump or Bailer ®/no) Type
Well Oiamcler: L-.Q In. Proleclive Posl/ Abulme~ /J) Concrele Pod {.;J;o)
(A) Top of Well Elevalion: ]]/. ]~ msl (yes/no) Well lnlegrify Solisfaclo (yes eno, explain below.
(B) Deplh lo Immiscible Layer. N/tff. Well Yield ( low / moderate high )
(C) Immiscible Layer Elevafion: (A)-(B)= l:,l d msl (yes/no)
(D) Depth lo Groundwoler. (8. 80 fl. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(D)= 751. q ~ msl (yes/no) DIA. or PIPE (in.) VOLUME IN GAL/Ff.
1.0 0.041 (F) Tofol Well Deplh = bl ff. 2.0 0.163
'-l1. io 3.0 0.367 (G) Length of Wafer Column: (F)-(D)= f I. 4.0 0.653
(1' ~ 5.0 1.020 Cosing Volume = (G) x Volume in gal./ft.= gals. 6.0 1.470
ldethod of Well Evacuation v>11~ Slart Time: () '1,,2. ( TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOVE flGURES BY
q,,~ Time: 1!21] 3.8 LITERS/GALLON. Method of Sample Colleclion
Chain-of-Cusfody Form Started ({;.,l}o)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged (gallons) G,. q I -,,_ 9-'l._b., 7 1, ,_ ~J-1-.r
TTme (military) t)q-,, e, e,q~(. (')~.S, 1110-, /017 pH (S.U.) (.. 1 t.. L (. '-I f z. -
' J..f Sp. Cond. (umhos/ cm) J ?.r I ·,'Li / l, 1 /'LS" tvr--Waler Temp. ("C) I, ,, 11 /1 /-1
Odor (subjeclive)• I I I I I Turbidily (subjeclive)" . I ' I I I ' • (l)None (2)Slighf (3)Moderole (4)Slrong
" (1)Clear (2)Slighlly Turbid (3)1.!oderolely Turbid ( 4)Very forbid (S)Exfremely Turtid
Commenls/Observolions/Recommendalions: -----------------------
FORM COMPLETED BY: (i~ it, ]kV>" Jlt_
DATE: ~S£JL.U..L-ff{~f~ _'
D& r r orm48 (3/94)
000092
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D 1')/1 S ENGINEERS ARCHff[CTS FIELD DAT A LOG I FLBYD PLANNERS SCIENHSTS FOR GROUNDWATER SAMPLE COLLECTION/
CHARLESTON. GREENWOOD. COLUMBIA GROUNDWATER ELEVATION MEASUREMENTS A
Well No.: Cf.A -5~ 1 c----,----------,--'-----___:_:_:::_::..:::..:.:::±~
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Client: Titonq Source(,) of Well ID Map 10 Lobel <Qno)
Sile Name: She\b,,1 A). C. Job No.:6Ot!r5. 00 Well Completion: Profcclive Cosing ~o) flush (yes~
Dole: 7 · 7,1.i q q LWR submilled by: __ -_____ flush-Moun! Cover Seal lnlacf (yes/no) Locking Cap (yes/no)
Sampling Personnel: -~J:L·c,&,_.'--_::r,u:,.L011:k..,,·_,,_.,.,. __ .... m..,....____ locked al Arrival (lyno) Departure @o)
Si1e Personnel: ___ .._ ____________ _ I Well Casing (height above/depth below) ground: f ,_C
Casing Type (P~ (other) __________ _ Regulatory Personnel:._=:-~-------------
Weother Conditions: _ _._(~1 '~t_a_r ______ T emp.: 'i( S:
ff.
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Well Diameter: L ' C> In.
(A) Top of Well Elevalion: 8)4 ~ 78Z,-~st(yes/no)
(B) Depth lo Immiscible layer. Nfttt.
(C) Immiscible layer Elevation: (A)-(B)= A/ A msl (yes/no)
(D) Depth lo Groundwoler.. _____ ?J"-M+·-£:1.....,_\ ____ .=ff.
(£) Groundwofer Elevofion: (A)-(0)= 11n.1 L msl (yes/no)
{F) Tofol Well Depth= -------~'L.:..i..H ___ __:f.::.I.
(G) Length or Wafer Column: {F)-(D)=-----J/-1,_,,c...,.l_~.,___r_t.
Casing Volume = (G) x Volume in gal./fl.= ___ yL,.•....:'v::__,qccalccs.
Method of Well Evacuation -~P~v~s,._ __ Slort Time:
I.ref hod of Sample Collection ? ~
Chain-of-Custody Form Slorted~o)
Time:
/031
10:si
Dedicated ~ or Bailer G/no) Type __ · ____ _
Protective Posf/Abulmenl ~) Concrete Pod €/fno)
Well Integrity Solisfoclorvftv~s. no) If no, explain below.
Well Yield ( low / (n od~;;;;~ Y high )
WELL VOLUME DATA
DIA. OF PIP£ (in.) VOLUME IN GAL/fl.
1.0
2.0
3.0
4.0
5.0
6.0
0.041
0.163
0.367
0.653
1.020
1.470
TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOVE flGURES BY
3.8 LITERS/GALLON.
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I FIELD ANALYSES
Volume Purged (gallons)
I nme (military)
pH (s.u.)
Sp. Cond. (umhos/cm)
Wafer Temp. ("C) I Odor (subjecfive)•
Turbidity (subjective)"
1st Volume
3. "L.
1040
5 0
'.3 ''.} I 1
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• (!)None (2)Slighf {3)Moderale (4)Slrong
2nd Volume 3rd Volume 4th Volume 5th Volume
I D.i 9,
5, 0
,.,
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I " (!)Clear (2)Slighlly Turbid {3)Moderofely Turbid (4)Very forbid {S)Exlremely Turbid '----'--'---__:__:__:_~'-----'---'-'---'------'...:_____:__------
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Commenls/Observations/Recommendations: -----------------------
D& r Form48 (3/94)
000093
CNGlNHRS ARCHITECTS FIELD DAT A LOG D1'}/1S
FLOYD PLANNERS SCICNTISTS
CHARLESTON • GREENWOOD • COLUMBIA
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
Well No· P-Si ..
Clienf: J,'c,ang Source(s) of Well fO M0p ID lobet@no)
Site Name: S1itlb,,, ~}. c. Job No.: p0~·Jr5. 0 0 Well Completion: Proleclive Cosing ~no) flush (yes@
Oate: 7· 7.1_-:9q LWR submiffed by: -rtush-1.!ounl Cover Seal lntocf (yes/no} locking Cap (yes/no)
Locked al Arrival G,;tno) Deparlure ({;;;no) Sampling Personnel: "T-6. :r ~ok.·., !Tl '
Sile Personnel: -Well Cosing (height above/deplh below} ground: '2.. s-
Regulatory Personnel: -Casing Type (P~ (Other)
Weather Conditions: c,.lea, Temp.: 90 Dedicated Pump ,or Boiler (yes/no) Type
Well Diameter: 1...-0 In. Protective Posl/ Abutment {yes no Concrete Pod ({;;}no)
(A) Top of Well Elevolion: 1f38-1'2,. msl (yes/no) Well lnlegrit~ocfory yes/ o) If no, exploin below.
(BJ° Depth to Immiscible layer. N/tn. Well Yield low moderole / high )
(C) Immiscible Loyer Elevolion: (A)-(B)= 6.L 8 msl (yes/no)
(D) Deplh lo Groundwoler. . '/...t-j. / G, ti. WELL VOLUl,(E DATA
(E) Groundwater Elevation: (A)-(D)= J(o:'),qC, msl (yes/no) DIA. or PIPE (in.) VOLUME IN GAL/Tl.
1.0 O.D41 (r) Totol Well Depth = 5 9. 0 ti. 2.0 0.163
3 3. ~:I 3.0 0.367 (G) length of Waler Column: (r)-(D)= f I. 4.0 0.653
5-~ 5.0 1.020 Cosing Volume = (G) x Volume in goi./11.= gals. 6.0 1.470
Method of Well Evacuation Bi~ Start Time: 1)1~ TO CONVERT GAL/TT TO LITERS/TT, l,(ULTIPLY ABOVE rtGURES BY
£11~ Time: /2, ()!;"
3.8 LITERS/GALLON. Method of Sample Collection
Choin-of-Cuslody Torm Storied {fr9-no}
FIELD ANALYSES sq "'fl /-t,
Volume Purged (gallons)
nme (military)
pH (S.U.)
Sp. Cond. (umhos/cm}
Waler Temp. (•c)
Odor (s_ubjeclive}'
Turbidity (subjective)"
1st Volume
~-)
/ J 7.,u
{..;
t7?
70
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• (!)None (2)Slighl (3}Moderole (4)Slrong
2nd Volume 3rd Volume 4th Volume
/I /T/1~71,)
11,0
e,,)
/, 7 c.
?0
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" (!)Clear (2)Slighlly Turbid (3)1.!oderolely Turbid (4}Very Turbid (5}Exlremely Turbid
0 . (Y) (I\(\ "
FORM COMPLETED BY:
DATE:
000094
15th Veldmo -I~"' -(,
[ I,, u
. 1JJ
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O& r form48 (3/94)
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: ;1~'"'~~:. ::: FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
I Well No.: .J: TE f-
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Clienl: Jj• f DD i ________ IO label (yes/no)
Stte Nome: )b I J b, 1 Alf, Job No.: 6 Ct,?g$: M
Ocrle: 7/7,7 /'lj LWR submilled by: __ -____ _
Well Compl ion: Prolective Cosing (yes/no) nush (yes/no)
ver Seal lntocl (yes/no) Locking Cop (yes/no)
Sampling Personnel: ::S-&--S...Jl,'rs I ot Locked at Arrivo yes/no) Departure (yes/no)
Site Personnel: ________________ _ Well Cosing (heighl ove/deplh below) ground: _____ -1L..
Regulatory Personnel: ______________ _ Cosing Type (PVC) (Slee (Other) _________ _:_
Weolher Condilions:. __ ,.f"'-,,,_Je_.4,_r -~----Temp.: ~ 5' Dedicated Pump or Boiler es/no) Type
Well Oiameter.._,/\_,_/,,,'1.,___,._A-'1glilp/Lh~· c..,q,.,_kl.,.r __ in. Protective Posl/ Abulmenl (yes/ Concrele Pod (yes/no)
(A) Top of Well Elev _________ msl (yes/no) Well Integrity Solistoctory (yes/no) no, explain below.
ft.
____ msl (yes/no)
(0) Depth to Groundwater. ft.
(E) Groundwater Elevation: (A) (OJ= ______ msl (yes/no)
(f) Total Well Depth = ft.
(G) lenglh of Water Column: (f)-( ft.
Cosing Volume = (G) x Volume in go gals.
Method of Well Evacuation _____ ..,_ Start Time: J ?iZ, 0
Method of Sample 'collection--~ __ _,__ Time: 11.30
Chain-of-Custody form Started ~no)
Well Yield ( low / moderole / high )
WEU VOLUME DATA
DIA. Of PIPE (in.) VOLUME IN GAL/fl.
1.0
2.0
3.0
4.0
5.0
6.0
0.041
0.163
0.367
0.653
1.020
1.470
TO CONVERT GAL/IT TO llTERS/IT. MULTIPLY ABOVE ncuRES BY
3.8 llTERS/GAUON.
FIELD ANALYSES
Volume Purged (gallons)
Time ( mililory)
pH (S.U.)
Sp. Cond. (umhos/cm)
Waler Temp. (•c)
Odor (subjective)•
Turbidity (subjective)"
1st Volume
• (1)None (2)Slight (3)Moderale (4)Slronge
2nd Volume 3rd Volume
" (l)cteor (2)Slightly Turbid (3)Moderalely Turbid (4)Very Turbid (5)Extremely Turbid
4th Volume •ijt oh:nrm" -17-:,,o
II-..._ I I!.,,
"-· ,no 1., u-,,.
I J LL
L,
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Comments/Observations/Recommendations: _1~\!,.,.,L'---_,/t,_..J~o~o~c-..,D,-=-t~c~c~:fr..,J~------------------
O& r rorm48 (3/94)
000095
CNC!NEERS ARCHITECTS FIELD DAT A LOG Di\)/1S
FLOYD PLANNERS SCIENTISTS
CHARLESTON • GREENWOOD " COLUMBIA
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
Well No · /(. z..e ..
Client: I,"cang Source(,) of Well ID M01? ID Lobel (yes/~
Sife Nome: 2h,\b,11 f:J c. Job No.: ti 0tl£5. 0 0 Well Completion: Protective Casing G/no) flush (yes/~
Oole: 7-ZJ.;~q LWR submifled by: -flush-Mounl Cover Seal lnfacl (yes/no) Lacking Cap (yes/ no)
Sampling Personnel: J,C,, -rt:ok,·•( II!. locked al Arrivol ~o) Oeporlure ~o)
Site Personnel: -Well Casing (heigh! abovi/deplh below) ground: t-f
Regulatory Personnel: -Casing Type (PVC) (Steel) (Other)
Weather Conditions: Glea. Temp.: qy-Dedicated ~ or Bailer (yes/no) Type
Well Diameter: l..0 · in. Proleclive Posl/Abulmenl ~) Concrete Pod (6}7no)
(A) Top of Well Elevation: &/f,? o msl (yes/no) Well lnlegril(9faclory (fj),o) If no, explain below.
(B) Depth lo Immiscible Layer. N/tft. Well Yield low / moderate / high )
(C) Immiscible Layer Elevation: (A)-(B)-6l /J msl (yes/no)
(o) Depth lo Groundwater. . l q_ 19 f I. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(0)= zq z .01 msl (yes/no) DIA. or PIPE (in.) VOLUME IN GAL/rt.
1.0 0.041
(r) Total Well Depth = z s. c) f I. 2.0 0.163
& J 8'1 3.0 0.367
(G) Lenglh of Waler Column: (r)-(0)= f I. 4.0 0.653
/ I Id 5.0 1.020
Cosing Volume = (G) x Volume in gol./fl.= gals. 6.0 1.470
Method of Well Evacuotion 2i1~ Start Time: 12S.?... TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOVE f!GURES BY 9,9 IBiD 3.8 LITERS/GALLON.
Method of Sample Collection Time:
Chain-of-Custody form Started -=-no)
FIELD ANALYSES
1st Volumo 2nd Volume 3rd Volume 4th Volume 5th Volume
Volume Purged (gallons) ,.~ 7,~7..,..,,\ -
nme (mililary) f '? ~ , I <.C}, !3? /\ .·.
pH (S.U.) r :'7 r.. _-4 -I ,,(,
Sp. Cond. (umhos/cm) '7 ,... ... ZT-i "J 7 ...
Waler Temp. ('C) Z.c . 7? Jq
Odor (subjeclive)• ,,. ' 'l.
Turbidity (subjective)" . -J., I -•
• (!)None (2)Slighl (3)Moderale ( 4)Slrong
" (l)Cleor (2)Slighlly Turbid (3)Moderolely Turbid (4)Very forbid (5)Exlremely Turbid
Commenls/Observo1ions/Recommendolions: __________________________ _
rDRM COMPLETED BY:
OAT[:
O& r form<B (3/9<)
000096
fl.
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D1')/1S
I FLOYD
[NCINEERS
PLANNERS
ARCHITECTS
SCIENTISTS
FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
I
STON • GREENWOOD • COLUMBIA Well No· 1/. e, ') ..
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Client: I,'e,ang Source(s) of Well IO f'.10f IO Lobel ~no)
Sile Nome: S 'li,\b,,1 t:il. c. Job No.: E 0th:5. 0 O Well Completion: Protective Casing ~no) flush (yes/;),
Dale: 7 · Z,,'L:j q LWR submitted . by: -flush-Moun! Cover Seal Intact (yes/no) Locking Cop (yes/no)
Sampling Personnel: J.C,. :r ,rnk,·•( lJ!. Locked al Arrival Q;no) Oeporlure r;::?no)
Sile Personnel: -Well Casing (height obov depth below) ground: J
Regulatory Personnel: -Casing Type (PVC)~(Olher)
Weather Conditions: Claoc Temp.: q 7 Dedicated Pump or Bailer ~/no) Type ·
Well Diameter: 7., • 0 In. Profecfive ~Abutment (yes/~ Concrete Pad ~no)
(A) Top of Well Elevalion: 111.r'! msl (yes/no) Well lnlegrily Salislaclory e}no) If no, explain below.
(Bf Depth lo Immiscible Loyer: NAtt. Well Yield ( low / moder~ /8
{C) Immiscible Loyer Elevation: (A)-(B)= 6l8 ms! (yes/no)
(0) Depth lo Groundwater. . /5.J..{O f I. WELL VOLUME DATA
{E) Groundwater Elevation: (A)-(0)= 72£ .J,f 'I msl (yes/no) DIA. or PIPE (In.) VOLUME IN .GAL/Fl.
1.0 0.041
{F) Total Well Depth = Z.2,!::l fl. 2.0 0.163
9, 3.0 0.367 (G) Length of Waler Column: (r)-{D)= f I. 4.0 0.653
1, 3 5,0 1.020 Cosing Volume = (G) x Volume in gol./11.= gals. 6,0 1.470
Method of Well Evacuation Bi~ Sforl Time: 1}35 TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOVE FIGURES BY
Method of Sample Collection ~. ,-" 13£1 3.8 LITERS/GALLON.
Time:
Chain-of-Custody Form Slorled {f?eyno)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged (gallons) I s 2... '-;,,q
Time (military) I -.., I , .,_,,,. / 2, c, -
pH {S.U.) c-. "' s-,, c; t -
Sp. Cond. (umhos/cm) L-, ZO {,,LJ&,0 I (, J A
Waler Temp. (•c) , ~ I "I I q
Odor (s.ubjeclive)• !.,I' '-l H
Turbidity {subjective),. • t I I
• (1)None {2)Slighl {3)Moderole {4)S1rong
" {1)Cleor {2)Slighlly Turbid {3)Moderolely Turbid (4)Very forbid (S)Exlremely Turbid
Commenls/Observafions/Recommendofions: -----------------------
FORM COMPLETE:A~:: ~;j; l~i: I uI
O& f form48 (3/94)
000097
{!,
.
DAJ.11S
fLOYD
ENGINECRS ARCHITECTS
PLANNCRS SCIENTISTS FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS CHARLESTON • GREENWOOD • COLUMBIA
Well No· C ( -2... 3 .. <
Client: J,"ce2ng Source{s) of Well ID M0p IO Lobel Q no)
Site Name: Shrlb-1 1 tJ C. Job No.: k Otfl:.S. 0 0 Well Completion: Prolective Casing. ~o) flush {yes~
Oofe: 7 · Z,1.: ~ q LWR submilled by: ffush-Mounf Cover Seal Intact {yes/no) Locking Cop {yes/no)
Sampling Personnel: J.C,, :rt: ok,·•( lIL Locked al Arrival ~no) oeParturc (;;;;no)
Site Personnel: -Well Cosing {heighf obove/depfh below) ground: z..s ft
Regulatory Personnel: -Cosing Type (P~C) ~) (Ofher)
Weather Condilions: Clef" Temp.: jJ Oedicoled tump, or Boiler ((;;/no) Type
Well Diameter: l.--0 In. Pro1ecfive Post/ Abutment (yes;Q Concrete Pad &,;I;no)
(A) Top of Well Elevofion: '&12. f,2:i msl {yes/no) Well Integrity Satisfactory Q~, explain below.
(B)' Oepth to Immiscible Loyer. N/tfl. Well Yield { low / moderate high
(C) Immiscible Loyer Elevofion: (A)-(B)= l:).ld msl (yes/no)
(D) Oepth to Groundwater. . l::1-l\ ft. WELL VOLUME OATA
(E) Groundwater Elevation: (A)-(D)= 1£lF1 1 S] msl (yes/no) DIA. or PIPE (in.) VOLUME IN GAL/rt.
.ss 1.0 0.041
(r) Total Well Depth = ft. 2.0 0.163
&.Z'.! 3.0 0.367 (G) Lenglh of Waler Column: (r)-(D)= fl. 4.0 0.653
I , ,<; 5.0 1.020 Cosing Volume = {G) x Volume in gol./tt.= gals. 6.0 1.470
Method of Well Evacuation P,,"@ Storl Time: H! ti TO CONVERT GAL/rT TO LITERS/rT, MULTIPLY ABOVE rtGURES BY
?. _.,., /'f'l.l
3.8 LITERS/GALLON. Method of Sample Collection Time:
Chain-of-Custody rorm Storled {<r;;;no) '
FIELD ANALYSES
' 1st Volume 2nd Volume 3rd Volume 4th Volume 5th Volume
Volume Purged (gallons) . ',' '-0 'f.' Time (mililory) fj. II/_ 1' z. /1-/ 7 l ....
pH (S.U.) /,., In '), ' t. -~
Sp. Cond. (umhos/cm) '.':,£I 3 ., ~ ..., ' (_ Waler Temp. ("C) I~ / B I~
Odor (subjective)• £.\ J.I
Turbidity (subjective}.,. . . I
• (l}None (2)Slighl (3)Moderole (4)Slrong
" (1)Cleor (2)Slighlly Turbid (3)Moderolely Turbid (4)Very forbid (5)Extremely Turbid
Commcnls/Obscrvofions/Recommendalions: ---------------------------
rDRM COMPLETED BY:
DATE:
D& r Form48 (3/94)
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ENGINEERS ARCHITECTS FIELD DAT A LOG
PLANH[RS sctnmsrs
CHARLESTON • GREENWOOD • COLUMBIA
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEV A TION MEASUREMENTS
Well No.: PF lu-1-J
Oale:_f--1-L.L4---l-2--LWR submillcd by: ______ _
Sampling Personnel: _:::S...>:..J-G"--'---. _::S...utC.1.Q\Ok.1Jj 115...,_, ......,IJL<=.... _____ _
Site Personnel: _______________ _
Regulatory Personnel: ______________ _
Weather Conditions: [, 1 PC!( Temp.: 9)
Well Diameter: b . C) In.
(A) Top of Well [levalion: 'kl-\8 • /'-, ms! (yes/no)
(B) Depth lo Immiscible Layer. fl.
(C) Immiscible Layer [levalion: (A)-(B)=_-_--::_ __ msl (yes/no)
(0) Depth lo Groundwaler. 3 4-] 3 ti.
([) Groundwoler Elevalion: (A)-(D)= &' ( 3, 1-\ \ ms! (yes/no)
(F) Tola! Well Depth = --------'CJ_3L.~3..L..-----'f"I.
(G) Lenglh of Waler Column: (F)-(D)= S 1j', S J fl.
Casing Volume = (G} x Volume in gal./ft.= __ ~72~=b~~go=ls.
Method of Well [vacualion ~ If MQ Start Time: / 1-j b ]
Method of Sample Collection ~1~ Time: / S: IC
Chain-of-Custody Form Started ~o)
. Source(s) of Well ID {hqp · ID Lobel Ef no)
Well Completion: Protective Cosing@o) f"lush (yes/@
flush-Mounl Cover Seal lnlacl (yes/no) Locking Cap (yes/no}
Locked at Arrival (yes;@ Departure (yes@
Well Casing (height above/depth below) ground: __ ~2,~ _ _,_tt ....
Casing Type (PVC) (Slee (Other} ___________ _
Dedicated Pump or Bailer (yes no) Type
____.1 Concrete Pad G-no)
Well Integrity Satisfactory explain below.
WELL VOLUM[ DATA
DIA. or PIPE (in.) VOLUME IN GAL/fl.
1.0 0.041 ~o Qt~
3.0 0.367
-1.0 0.653
5.0 1.020
~ 1.470
TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOVE FIGURES BY
3.8 LITERS/GALLON.
FIELD ANALYSES
Volume Purged (gallons)
Time (mililary)
pH (S.U.)
Sp. Cond. (umhos/cm)
Waler Temp. (•c)
Odor (subjective)•
Turbidity (subjective)"
71111.tl / !It.. 1
11,f 30
-0
~If
-":I
?
. I
• (!)None (2)Slighl (3)Moderale (4)Slrong
2nd Volume 3rd Volume
7q1"11>"7 ( ,., 'l. ) 't'l"l.74"' U-61
/J.ly 1 I,.: I A
6-I C. '
JI"], JJ,
?7 -? 7
? 7.
\ \
" (1)Cleor (2)Slighlly Turbid (3)Moderalely Turbid (4)Very forbid (5)Exlremely Turbid
41h Volume 5th Volume
-
Commenls/Observalions/Recommendalions: .,_Al=o--"/o,.,,.,ll,.__,_,n'.!,i)L___Ul,(,.J./:C,./ l-"'----J.hua,i,11c:\>.1i LlQl-'l~c'------------
0 -00 "'~ I I
FORM COMPLETED BY:
DAT[:
O& r form48 (3/94)
000099
D1\)/1S
FLOYD
ENGINEERS ARCHffEC'fS FIELD DAT A LOG
PLANNERS SCl[tHISTS
CHARLESTON • GREENWOOD • COLUMBIA
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
Well No· PEW -~ ..
.
Client: Ii"e,ang Source(,) of Well IO M •r ID Lobel 8no)
Sife Name: S1~\b,,1
t,). c. Job No.: Ji Oi:h:.S. 0 0 Well Complelion: Protective Cosing go} flush (yesB
Dole: 7-Z.,1.: 9 q LWR submilled by: -flush-1.founl Cover Seal lnfocl (yes/no) locking Cop (yes/ no)
Sampling Personnel: '}'.C,. :rt'. ok,·•( !I!. locked of Arrival {yes@ Departure (yes/~
Sito Personnel: -Well Cosing (heigh! o~ol'e/deplh below) ground: 2.... fl.
Regulatory Personnel: -Cosing Type (PVC)~Olher)
Weather Conditions: Clet>r Temp.: ~.S-Dedicated Pump or Bailer U!:fno) Type -Well Oiameler: C,, .o In. Proleclive Post/Abutment ~no) Concrete Pod ~no)
{A) Top of Well [levolion: f/tj 2-7-S-msl {yes/no) Well lnlegrify Solisfoclory {yes@o• exploin below.
(Bf Deplh to Immiscible Loyer. Nitti. Well Yield { low / moderate /i high
{C) Immiscible layer Elevofion: {A)-(8)= /.,l ti msl (yes/no}
{D) Depth to Groundwater. . ~7,S-1 ti. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(D)= ff//. ]t/ msl (yes/no} DIA. or PIPE (in.) VOLUME IN GAL/Ft.
1.0 0.041
(F) Total Well Oeplh = ~r f I. 2.0 0.163
3.0 0.367 (G) lenglh of Woler Column: (F}-(D)= s:l.:J~ f I. 4.0 0.653
~':1-1 5.0 1.020 Cosing Volume = {G) x Volume in gol./fl.= gals. 6.0 1.470
Method of Well Evacuation ev~ Siert Time: I 5-?,'--TO CONVERT GAL/FT TO LITERS/FT. MULTIPLY ABOVE flGURES BY p /6QI
3.8 LITERS/GALLON.
Method of Sample .Colleclion Time:
~no)
•
Chain-of-Custody Form Started
I 0080'1 FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 5th Volume
Volume Purged (gallons} Jrhn,n r o.s-, In I n,,-1 I ._,...,) 11111'2."I /-....-\
Time {mililory) I <.,j 1 IL·-I • .
I 61.-7
pH (S.U.) 1.0 7, I C, <\ -
Sp. Cond. (umhos/ cm} "-~ C, 1 <: 1-l
Waler Temp. (•c) 1? 1 :? 1,..;
Odor (subicclivc)' 1.. 7_ 'l
Turbidity (subjective) .. -I I '
• {!)None (2)Slighl (3}Moderole {4)Sfrong
" (1)Clcor (2)Slighlly Turbid (3}Moderolely Turbid {◄}Very forbid (5}Exlremely Turbid
Commenls/Obscrva1ions/Recommendalions: (ta /l ~ !,fpltcd-sli.A 1,..(\ ' I "ill 4~\:i d .,, :l:g 1, ... 1 \
JR(,' o.p0 m~/,_,1 _________________ ___,.,.._-11c-J1------
roRM COMPLETED sr, TI)j, 1t;,J-;; . ,rr
ff I th/""""'"' , DATE: 7 2-7,, 19
O& r form48 (3/94)
000100
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Df\YIS
IFLOYD
ENGINEERS
PLANNERS
ARCHITECTS
SCIENTISTS
FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS 1·
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CHARLESTON • GREENWOOD • COLUMBIA
., Well No· Pew-1
Client: T,u2!19 Source(s) of Well ID M0p 10 Lobel @no)
Sile Nome: S)i,\b,,1 ~1-c. Job No.: '1 Ot&:.S. o o Well Completion: Protective Cosing ~no} flush (yes@
Dale: 7· Z.:}·jq LWR submilfed by: -ffush-t.founf Cover Seol fnfocf (yes/no) locking Cap (yes/no)
Sampling Personnel: -r. e,, :r t:ok1'•( II!. Locked of Arrivof ~ Deparlurc ~
Sile Personnel: -Well Cosing (height above/depth below) ground: / • L
Regulatory Personnel: -Casing Type (;;) g (other)
Weather Conditions: c..t~lk--Temp.: 1~ Dedicated Pump or Baile~/no) Type ·
Well Diameter: ~-0 In. Proleclive P~bulment (yes no) Concrefe Pad Qno)
(A) Top of Well [fevafion: ~46-bS-msl (yes/no) Well ln1egrity Salisfoclory (yesf@f no, explain below.
(B)" Depth to Immiscible Loyer. N/tH. Well Yield ( low/ moderate /8
(C) Immiscible layer [lr,vafion: (A)-(B)= 6.l d msl (yes/no)
(D) Depth lo Groundwoler. . /.JS. -z._3 11. W[ll VOLUt.f[ DATA
([) Groundwater Elevation: (A)-(D)= Bl'2l•/.,L msl (yes/no) DIA. or PIPE (in.) VOLUME IN GAL/ff.
~ 1· 3 1.0 0.041
(f) Total Well Depth = ff. _b9-. 0.163
l_:j b,oJ 3.0 0.367
(G) Length of Wofer Column: (f)-(D)= ff. 4.0 0.653
6 2· 1 5.0 1.020 Casing Volume = {G) x Volume in gol./11.= gals. 6.0 1.470
Method of Well Evocuafion ev .. ~ Sfarl Time: I S:1.-1 '7 TO CONVERT GAL/n TO LITERS/FT, MULTIPLY ABOVE ffGURES BY
D, "'" lf.~5 3.8 LITERS/GALLON.
Method of Sample Collection Time:
'
Chain-of-Custody form Storied ~1no)
sl~')/\','i FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 5th Vofumo
Volume Purged (gallons) l-.10i11r7 I ~ei.l 'l.7'f1'170 -1'~ 1 no 7"'1(' / 1.0111
Time (mililory) /L : \ Ii::,-.,
pH (S.U.) 'i. s. ~ -
Sp. Cond. (umhos/cm) " -ss-
Wafer Temp. ("C) 7 I t.l
Odor (s_ubjecfive)• fr H
Turbidity (subjective)" . I I
• (l)None (2)Slighf (3)Moderafe (4)Sfrong
" (l}Cfeor (2)Slighfly Turbid (3)Moderolely Turbid (4)Very forbid (5)Exfremely Turbid
Commenls/Observalions/Recommendalions: ~UJ=• cll_..,~_l/.u>1..,' ~'\-uhDwc<,__._,rv,"-_,_/,,wCut'..c•c._ ___________ _
000101
fORM COMPL[TED BY: 1-~ · ~ I llr
DATE: 7 '2,'1;_
O& r form48 (3/94)
!I.
DAJIIS
.FLOYD
ENGINEERS ARCHITECTS FIELD DAT A LOG
PLANNCRS SCIENTISTS
CHARLESTON • GRECNWOOO • COLUMBIA
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
Well No · F, 5 c; .. ~--
Clienl: J,'e,ona Source(,) of Well ID Mep ID label (y;,e
Sile Nome: Sh,\h,,1 t,,).C. Job No.: t1 Otll:5. o o Well Completion: Prolcclivc Cosing ~no} flush (yes/e!:,
Dale: 7-L,1.: ~ q LWR submilled by: -flush-Moun! Cover Seal Intact (yes/no) Locking Cap (yes/ no)
Sampling Personnel: "}".C,. "J t'.CllG•( . II!. Locked of Arrival (yesW Dcparlurc (yes/(;?
Sile Personnel: -Well Casing (height above/depth below) ground: t-/
Regulatory Personnel: -Casing Type (PVC) (Steel) (01her)
Weather Conditions: C-/u.r Temp.: o/'l Dedicated Pump or Bailer ~no) Type
Well Oiamcfer: 'L.. 0 In. Protective Post/Abutment 9-\0) Concrete Pod G;,/no)
{A) Top of Well [levofion: f2!:i 9 , 13 ms! {yes/no) Well Integrity Solisfaclory (yes,@ If no, explain below.
(B)" Depth to Immiscible Layer: NA-ft. Well Yield ~ moderate / high )
(C) Immiscible Loyer Elevation: {A)-(B)= f.,l /J ms! {yes/no)
{D) Depth lo Groundwater: . 3 g_ 7,'-, fl. WELL VOLUME DATA
{E) Groundwater Elevation: {A)-(D)= o-10, 1 3 ms! (yes/no) DIA. Of PIPE {in.) VOLUME IN GAL/fl.
1.0 0.041
{F) Talat Well Depth = r::. C. f I. 2.0 0.163
3.0 0.367
{G) Length of Waler Column: (F)-(D)= I 0 • 7 !::I f I. 4.0 0.653
5.0 1.020 Casing Volume = {G) x Volume in gat./ft.= l.7 gals. 6.0 1.470
Method of Well Evacuafion e~,,11ci 5lar1 Time: l r.s: :J TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOV[ FIGURES BY
0 -~I'\ I 'JI~
3.8 LITERS/GALLON.
Method of Sample Collection Time:
Chain-of-Custody r orm Storied (resJ no)
1st Volume >q1!~ :~E~" ANALYSE3:d Volume 4th Voluma 5th Volume
Volume Purged (gallons) TO" , v
nme {military) It. I 0
pH (5.U.) l..lJ
Sp. Cond. (umhos/cm) 1. (,,'
Waler Temp. (•c) 1 t,
Odor {subjeclive)' J.I
Turbidity {subjeclive)" -I
• (!)None {2)51ighl (3)Moderale (4)Slrong
" (!)Clear (2)5tighlly Turbid (3)Moderalely Turbid
Comments/Observalions/Recommendalions: )o/91.e,
w~d ... coD nii n•U2 ;,!) k11111a-:I·~,
~
1'1/1-1
I,,·°'
!, '} ...,
"/.1
/./
I
( 4)Very forbid {5)Exfremely Turbid
Free
Alo
Pc,J,c
lark 011
obv ""k "'l-e"~ 1wl1 u<tn .
000102
-
.
D& F form48 (3/94)
(f.
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Master Tracking List
Sample ID
L99072310-0l
Field Data
EPA 170.1
SW846 9040B
SW846 9050
Client
Contact
Volatile Organics
SW846 8260B
L99072310-02
Field Data
EPA 170.1
SW846 9040B
SW846 9050
Volatile Organics
SW846 8260B
L99072310-03
Field Data
EPA 170.1
SW846 9040B
SW846 9050
Gas Chromatography
SW846 8015
Volatile Organics
SW846 8260B
Wet Chemistry
SWB46 9060
L99072310-04
Field Data
EPA 110.1
SW846 9040B
SW846 9050
TICONA, LLC
P.O. BOX 87
SHELBY, NC 28151-0087
JERRY MCMURRAY
Client ID
HH-77
HH-48
ITCI
C-49
NC Certification Number: 25
Project Number: 60885.00-0003
Report Date
Page 1 of 7
September 17, 1999
Date Collected
21-JUL-99 12:00
21-JUL-99 12:06
21-JUL-99 12:50
21-JUL-99 14:19
000103
Date Received
23-JUL-99
07/21/99 1200
07/21/99 1200
07/21/99 1200
07 /27 /99 0953
23-JUL-99
07/21/99 12 06
07/21./99 1206
07/21/99 12 06
07/27/99 1013
23-JUL-99
07/21/99 1250
07/21/99 1250
07/21/99 1250
08/02/99 1712
07/27/99 1034
07/26/99 1132
23-JUL-99
07/21/99 1419
07/21/99 1419
07/21/99 1419
Davis & Floyd, Inc. ! PO Drawer 428 \ Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I {864) 229-4413 j Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
NC Certification Number: 25
Master Tracking List
Client TICONA, LLC Project Number: 60885.00-0003
P.O. BOX 87
SHBLBY, NC 28151-0087 Report Date September l 7, 1999
Contact JERRY MCMURRAY Page 2 of 7
Sample ID Client ID Date Collected Date Received
Volatile Organico
SW846 8260B 07/27/99 1054
L99072310-05 T-35 21-JUL-99 15:26 23-JUL-9!:J
Field Data
EPA 170 .1 07/21/99 1526
SW846 9040B 07/21/99 1526
SW846 9050 07/21/99 1526
Volatile Organics
SW846 8260B 07/27/99 1114
L99072310-06 EE-58 21-JUL-99 16:11 23-JUL-99
Field Data
EPA 170.1 07/21/99 1611
SW846 9040B 07/21/99 1611
SW84G 9050 07/21/99 1611
Volatile Orga.nica
SWB4G 8260B 07/27/99 1135
L99072310-07 FF-34 21-JUL-99 17:16 23-JUL-99
Field Data
EPA 170. 1 07/21/99 1716
SW846 9040B 07/21/99 1716
SW846 9050 07/21/99 1716
Volatil(? Organic&
SW846 8260B 07/27/99 1155
L99D72310-08 FF-62 21-JUL-99 17: 25 23-JUL-99
Field Data
EPA 170.1 07/21/99 1725
SW846 9040B 07/21/99 1725
SW846 9050 07/21/99 1725
000104
Davis & Floyd, Inc. I PO Drawer 42B I Greenwood, SC 2%4U I 816 [. Durst Avenue ! Greenwood, SC 29(,49 I [phone] I fax (U(,4) 229-7119
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Df\YIS
FLOYD LABORATORY ANALYSIS REPORT
Master Tracking List
Client
Contact
Sample ID
Volatile Organics
SW846 8260B
Field Data
EPA 170.1
SWB46 9040B
SW846 9050
Volatile Organics
SW846 8260B
L990723l.0-10
Field Data
EPA 170.1
SW846 9040B
SW846 9050
Volatile Organics
SW846 8260B
L99072310-ll
Field Data
EPA 170.l
SW846 !1040B
SW846 9050
Volatile Organics
SW846 8260B
L9!1072310-12
Field Data
EPA 170.l
SW846 9040B
SW846 9050
TICONA, LLC
P.O. BOX 87
SHELBY, NC 28151-0087
JERRY MCMURRAY
Client ID
G0-61
AA-54
P-58
ITEF
NC Certification Number: 25
Project Number: 60885. 00-0003
Report Date ' September 1 7, 1999
Page 3 of 7
Data Collected Date Received
07/27/99 1216
22-JtrL-99 10: 17 23-JUL-99
07/22/99 1017
07/22/99 1017
07/22/99 1017
07/27/99 123 6
22-JUL-99 10: SB 23-JUL-99
07/22/99 1058
07/22/99 1058
07/22/99 1058
07/27/99 1257
22-JUL-99 12:05 23-JUL-99
07/22/99 1205
07 /22/99 12 05
07/22/99 1205
07 /27 /99 1422
22-JUL-99 12:30 23-JUL-99
07/22/99 1230
07/22/99 123 0
07/22/99 1230
000105
Davis & Floyd, lnc. \ PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 ! (8(,4) 229-4413 I fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Master Tracking List
client
Contact
Sample ID
Gae Chromatography
SW846 8015
Volatile Organics
SWB46 8260B
Wet Chemiatry
SW846 9060
L99072310-13
Field Data
EPA 170.
SW84.6 9040B
SW846 9050
Gae Chromatography
SW846 8015
Volatile Organicn
SW846 8260B
Wet Chemistry
SW846 9060
L99072310-14
Field Data
EPA 170.1
SW846 9040B
.''JW84G 9050
Volatile Organics
SWB46 8260B
Wet Chemistry
SW846 9060
TICONA, LLC
P.O. BOX 87
.SHBLBY, NC 28151-0087
JERRY MCMURRAY
Client ID
ITEF DUP.
K-28
NC Certification Number: 25
Project Number: 60885.00-0003
Report Date September 17, 1999
Page 4 of 7
Date Collected
22-JUL-99 12:30
22-JUL-99 13:20
000106
Date Received
08/02/99 1226
07/27/99 1443
07/26/99 1149
23-JUL-99
07/22/99 1230
07/22/99 1230
07/22/99 1230
oa/02/99 1249
07/27/99 1503
07/26/99 1330
07/22/99 1320
07/22/99 1320
07/22/99 1320
07/27/99 1524
07/26/99 1349
Davi:,; & floyd, Inc. I l'O Drawer 428 I Greenwood, SC 2%48 I HH, E. Durst Avenue I Greenwood, SC 2%49 I (864) 229-441} I fax [phone]
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
NC Certification Number: 25
Master Tracking List
Sample ID
L99072310-1S
Field Data
EPA 170.1
SW846 9040B
SW846 9050
Client
Contact
Volatile Organics
SW846 8260B
Wilt Chemistry
SW846 9060
L99072310-16
Field Data
EPA 170.1
SW846 9040B
SW846 9050
Volatile Organics
SW846 8260B
L99072310-17
Field Data
EPA 170.1
SW846 9040B
SW846 9050
Semivolatile Organics
SW846 8270C
SW846 8270C OOWTHERM
Volatile organics
SW846 8260B
L99072310-18
Field Data
EPA 170 . .1
SW846 9040B
Davi~ & Floyd, Inc. I PO Drawer 428
TICONA, LLC
P.O. BOX 87
SHELBY, NC 28151-0087
JERRY MCMURRAY
Client ID
V-23
CC-33
PEW-4
07 /27 /99
07/27/99
PEW-4 DUP.
Project Number: 60885.00-0003
Report Date
Page 5 of 7
September 1 7, 1999
Date Collected Date Received
22-JUL-99 13:57 23-JUL-99
07/22/99 1357
07/22/99 1357
07/22/99 1357
07/27/99 1849
07/26/99 1410
22-JUL-99 14:27 23-JUL-99
22-JUL-99 15:15
0830
0830
22-JUL-99 15: 15
07/22/99 1427
07/22/99 1427
07/22/99 1427
07/27/99 1605
23-JUL-99
07/22/99 1515
07/22/99 1515
07/22/99 1515
08/03/99 1222
08/06/99 1011
07/27/99 162 6
23-JUL-99
07/22/99 1515
07/22/99 1515
000107
Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-441) I Fax [phone]
-"!'
DAYIS
FLt1YD LABORATORY ANALYSIS REPORT
NC Certification Number: 25
Master Tracking List
Cont,1ct
Sample ID
SW846 9050
Semivolatile organics
SW846 B270C
SWB46 8270C DOWTHERM
Volatile Organicn
SW846 8260B
L99072310-19
Field Data
EPA 170.1
SW846 9040B
SWB46 9050
Semivolatile Organics
SWB46 8270C
SWB46 B270C DOWTHERM
Volatile Organics
SW846 8260B
Field Data
EPA 170.1
SWB46 9040B
SWB46 9050
Semivolatilo Organice
SW846 8270C
SW846 8270C DOWTHERM
Volatile Organics
SW846 8260B
L99072310-21
Fiold Data
EPA 1 70. 1
SW846 9040B
TICONA, LLC
P.O. BOX 87
SHELBY, NC 28151-0087
JERRY MCMURRAY
Project Number: 60885.00-0003
Report Date
Page 6 of 7
September 17, 1999
Client ID Date Collected Date Received
PEW-3
PEW-1
F-55
07/27/99 0830
07/27/99 0830
22-JUL-99
07/27/99 0830
07 /27 /99 0830
22-JUL-99
07/27/99 0830
07/27/99 0830
22-JUL-99
000108
07/22/99 1515
08/03/99 1300
08/06/99 1048
_07/27/99 1647
16:24 23-JUL-99
07/22/99 1624
07/22/99 1624
07/22/99 1624
08/03/99 1339
08/06/99 1124
07/27/99 1707
16:55 23-JUL-99
07/22/99 1655
07/22/99 1655
07/22/99 1655
08/03/99 1417
08/06/99 1200
07/27/99 1728
17: 14 23-JUL-99
07/22/99 1714
07/22/99 1714
D,wis & Floyd, Inc. I PO Drawer 428 ! Greenwood, SC 2%411 I Bl & E. Durst Avenue I Greenwood, SC 29649 I [phone] I rax (B(,4) 229-7119
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DAJ!IS
FLOYD LABORATORY ANALYSIS REPORT
NC Certification Number: 25
Master Tracking List
Client
Contact
Sample ID
SW846 9050
Semivolatile Organics
SW846 8270C
SW846 8270C DOWTHERM
Volatile Organics
SW846 8260B
L99072310-22
Volatile organics
SWB46 8260B
TICONA, LLC
P.O. BOX 87
SHELBY, NC 28151-0087
JERRY MCMURRAY
Project Number: 60885.00-0003
Report Date
Page 7 of 7
Sept.ember 1 7, 1999
Client ID Date Collected Date Received
TRIP BLANK
07/27/99 0830
07/27/99 0830
21-JUL-99 06:30
000109
07/22/99 1714
08/03/99 1455
08/06/99 1541
07/28/99 0915
07/28/99 1158
Davis & Floyd, Inc. I PO Drawer 42B I Greenwood, SC 29648 l 816 L Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
August 23, I 999
JERRY MCMURRAY
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
Login Number
Project Number
Description
:L99081903
:60885.00
:GROUNDWATER
Dear Jerry Mcmurray:
. We are pleased to provide the enclosed analytical results for the samples received by
Davis & Floyd, Inc. on August 18, 1999.
A formal Quality Assurance/Quality Control program is maintained by Davis & Floyd,
which is designed to meet or exceed the EPA or appropriate regulatory requirements.
All analytical analyses for this project met QA/QC criteria unless otherwise stated in the
footnotes. This report is to be reproduced only in full.
Feel free to contact our Client Services Representative at [phone] if further
explanation of the analysis is required. Unless other arrangements have been made, samples
will be disposed of or returned f4 days from the date of the report. We appreciate the
opportunity to provide services to your firm.
Sincerely,
DA VIS & FLOYD, INC.
1;;;1
J n 1-1. McCord, Jr.
aboratory Manager
00011n
Davis & Floyd, Inc. I PO Drawer 428 j Greenwood, SC 2964B I 816 L Durst Avenue I Greenwood, SC 29649 I [phone] I Fax (B(i4} 229-7119
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITEF
Matrix
Parameter
Gas Chromatography
SW846 8015
ETHYLENE GLYCOL
GW/ChemW
NC Certification Number: 25
Result
Project Number: 60885.00
Report Date
Page 1 of 1
Sample ID
Auguot 23, 1999
L99081903-0l
Date Collected: lB-AUG-99 11:45
Date Received 18-AUG-99
Qual RDL Units lmalyst Date Time
7.0 7.0 JAW 08/23/99 0828
0()()1.11
Davis & Floyd, Inc. I PO Drawer 428 ! Greenwood, SC 2%48 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITEF DUP.
Matrix
Parameter
Ga& Chromatography
SW846 8015
BTHYLENE GLYCOL
GW/ChemW
NC Certification Number: 25
Project Number: 60885.00
Report Date Auguot 23, 1999
Page l of l
sample ID L99081903-02
Date Collected: 18-AUG-99 11 : 45
Date Received 18-AUG-99
Reault Qual RDL Units Analynt Date Time
7.0 7.0 mg/1 JAW 08/23/99 0855
000112
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2%48 ! 816 E. Durst A_venue I Greenwood, SC 29649 j [phone] I Fax {864) 229-7119
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA,LLC
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITCI
Matrix
Parameter
Gas Chromatography
SW846 8015
ETHYLBNE GLYCOL
GW/ChemW
NC Certification Number: 25
Project Number: 60885.00
Report Date Auguot 23, 1999
Page 1 of 1
Sample ID L990B1903-03
Date Collected: 18-AUG-99 11 ;50
Date Received 18-AUG-99
Result Qual RDL Units Analyst Date Time
250 7.0 mg/1 JAW OB/23/99 0923
I Davis & Floyd, Inc.
000113
I PO Drawer 428 ! Greenwood, SC 29648 1 816 L Dursl Avenue I Greenwood, SC 2%49 I [phone] I Fax (8f,4) 229-7119
DAJ!IS
FLtlYD LABORATORY ANALYSIS REPORT
Master Tracking List
Client
Contact
Sample ID
Gae Chromatography
SW846 8015
Gas Chromatography
SWB46 8015
L99081903-03
Oas Chromatography
SW846 8015
TICONA, LLC
P.O. BOX 87
,SHELBY, NC 28151-0087
JERRY MCMURRAY
Client ID
ITEF
ITEF DUP.
ITCI
NC Certification Number: 25
Project Number: 6088S.00-0003
Report Date September 21, 1999
Page 1 of 1
Date Collected Date Received
18-AUG-99 11:45 18-AUG-99
08/23/99 0828
18-AUG-99 11 :4S
08/23/99 0855
18-AUG-99 11: 50 18-AUG-99
08/23/99 0923
000114
Davis & Floyd, Inc. I PO Drawer 42H I Grt!(!nwood, SC 2%411 I Bl f> L Dur~1 Avenue I Greenwood, SC 2Wi49 I {Bf,4) 229-441 J I fax (ll(i4) 22')-711 ~J
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Method Conformance Summary
Client: HNA HOLDINGS, INC
Login: L99081903
Criteria Volatiles
Sample Holding Time
Standards Preparation
Instrument Tuning
Instrument Calibration
Calibration Verification
Degradation Check
Interference
Sample/Standard
Blanks Results
Method Accuracy
Method Precision
Surrogate Recovery
PDS/SD/MSA
TCLP Preparation
Key ✓
NIA
= Met Criteria Met
= Not Applicable
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
Semi
Volatiles
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
Metals
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
*
PDS =
SD =
MSA=
Method Criteria Not Met -Seefootnote(s) below.
Post Digestion Spike
Serial Dilution
Method of Standard Additions
Footnotes: Ethylene glycol is summarized under "Other" column.
Project Number: 60885.00-0000
Report Date: August 23, 1999
Inorganics Other
NIA ✓
NIA v
NIA NIA
NIA ✓
NIA ✓
NIA NIA
NIA NIA
NIA ✓
NIA v
NIA ✓
NIA NIA
NIA NIA
NIA NIA
Ethylene glycol results represent re-analysis of samples originally included in
L99072310.
000115 I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2%48 I Ill 6 E. Durst Avenue I Greenwood, SC 2%49 I [phone] I rax [phone]
"DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Master Tracking List
client
Contact
Sampl,, ID
L99081903-0l
Gao Chromatography
SW846 8015
Gaa Chromatography
SW846 8015
L99081903-03
Gas Chromatography
SW846 8015
TICONA,LLC
P.O. BOX 87
.SHELBY, NC 28150
JERRY MCMURRAY
Client ID
ITEF
ITEF DUF.
NC Certification Number: 25
Project Number; 60885.00
Report Date
Page 1 of 1
Auguot 23, 1999
Date Collected Date Received
18-AUG-99 11:08 18-AUG-99
08/23/99 0828
18-AUG-99 11:08 18-AUG-99
08/23/99 0855
18-AUG-99 11:08
08/23/99 0923
000116
Davis & r-loyd, Inc. I PO Drawer 4211 I Greenwood, SC 29(,4fl I 8H) (. Durst Avenue I Greenwood, SC 2%49 \ (8(,4) 229-4413 I fax [phone]
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DAYIS
FLbYD LABORATORY ANALYSIS REPORT
Method Blanks
Blank
Parameter
Oas Chromatography
SWB46 8015
ETHYLENE GLYCOL
HB18656:l
I Davis & Floyd, Inc. I PO Drawer 428 J Greenwood, SC 2%48
Report Date
Page 1 of 1
Matrix
August 24, 1999
GW/ChemW
WorkGroup: WG18656
Cone Qual ROL Units Analyst Date Time
7.0 7.0 JAW 08/23/99 0800
000117 I 816 f.. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax[phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Laborato,y Control Standards and Duplicates
LCS : LCS18656:1
ETHYLENE GLYCOL 50. 00 47.06
Report Date : Auguot 26, 1999
Page 1 of 1
Matrix ; GW/ChemW
WorkGroup: WG18656
Method : SW846 8015
94.1 64-117
000118
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Davis & Floyd, Inc. I l'O 0r;iwer 428 I Greenwood, SC 2%4B I 816 E. Durst Avenue I Greenwood, SC 29(149 I [phone] I fax [phone] I
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
ETHYLENE GLYCOL
:Parameter
8THYLENE GLYCOL
Matrix Spikes and Duplicates
MS/MSD MS99081903-0l:18656
MSD99081903-0l:18656
··s't·i_·k~
.A<ld_~·4)-·,
50. 00
50. 00
< 7.00
50 .35
Report Date
Page 1 of
Augunt 26, 1999
Matrix GW/ChemW
WorkGroup: WG18656
Method
55.06
104. 9
SW846 8015
·.\R?C
110 .1
::\RPD-
4. 05
73-116
20 73-116
000119 I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue l Greenwood, SC 29649 I [phone] ! Fax [phone]
------

-

-
----

-
--D~IS iqile,rill 1rcilt!du,
FL YD -~-!mi"' Chain of Custody Record
Cffent Project I Site Location 816 E. Durst Avenue, Greenwood, SC 29649 [phone] Fax: [phone]
TICONA 60885.00. Laboratory Cerlifcalion Numbers: SC· 24110, NC-25, TN· 2923, VA· 77
SHELBY,NC
Contact Report To Copy To Reporting Requirements: [ J Standard [ J Data Package (Specify Level)
Johnny Ledford
Collected By Required Parameters, Containers end PreseNatives
.C:, C, cti~CL. r::ra.. " E 0 ~
NOTICE: " e § 0
:s >: ·§
8 ~" C 0 .S o C) ~ .... .~ 0 " E~ • : 8. 8. 6 C
~ s ~ 0 • E E E " Sample Collection ~ _§_ 8 e • , 5 " " z w
Samole Descriotion Date Time Time Type Total A
"J:.'Ti::-F g -Ix.,;/() l;/J~< V " 1TC. ~ -bw> ,C,../b .• ('< II'"-< ~ t.
TTCI f:/A1.W ll· iso
., 2-
R~& , ,/,. Date Time Reliquished By Date Time Re/iquished By Date Time
c-£9(> v'6r 3:'.,
Received /jy -Date Time Received By Date Time
;;,v;: Lam/~11;~ y t"~ Date Time
,9./R. QG /1,.30
1r.;omments
Matrix Type Definitions 1 -Drinidng Water 2 • Clean Water 5 • Groundwater 7 -Soil/Sediment 8 • Liquid Sludge g. Oil 12 -Alr
Preservative Definitions A-None 8-H2S04 C-HCI D • HN03 E • NaOH F • Filtered G-Other
--

-
-Page ----L of_/ __
,ce use vnly
Purchase Order
State Quote
NC
LOyln Special Instructions
«"I :,
! i~ 0 • C N ~ . >, ~
Cb ii '6 ~
...J .s
Fraction HOT ..... ommems
OJ
0)...
03
Quick TAT Ship~y
y 8 w ~ENT
"' f[DE)(
If/city: Aitbi/1 Number
--'"'
Coolo,ID~ablo), /
Oo '''" Ye o Temp(C:,--b
Custody Seal: Intact I Broken Non~
Davis & Fsayr;, Inc.
FL02_01 (02/'i/9)
C
C'J ....,
0
0
0
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DA,YIS
FLtJYD LABORATORY ANALYSIS REPORT
Explanation of Symbols and Abbreviations
The following defines common symbols and abbreviations used in reporting technical data:
RDL Report Detection Limit MDL Method Detection Limit
TOP Top of Pipe MSL Mean Sea Level
TNTC Too Numerous To Count MPN Most Probable Number
BTU British Thermal Units NTU Nephelometric Turbidity Units
C Degrees Centigrade F Degrees Fahrenheit
umhos/cm micromhos/cm meq milliequivalents
kg kilogram ls) g gram(s)
mg milligram ls) ug microgram(s)
I literlsl ml milliliters(s)
ul microliter(s) m3 cubic meter(s)
lb pound(s) ft3 cubic foot(feet)
ft foot(feet) TIC Tentatively Identified Compounds
mg/I, mg/kg Units of concentration in milligrams per liter for liquids and milligrams per kilogram for solids.
Also referred to as Parts Per Million or "ppm" when the assumption is made that the specific
gravity or density is one (1 g/ml).
ugn, ug/kg Units of concentration in micrograms pe~ liter for liquids and micrograms per kilograms for
solids. Also referred to as Parts Per Billion or "ppb" when the assumption is made that the
specific gravity or density is one ( 1 g/ml).
wt% Units of concentration expressed on a weight/weight basis (e.g. grams per 100 grams).
< Less Than -The number following the sign is the limit of quantitation, the smallest amount of
analyte that can be reliably determined using this test.
> Greater Than
Data Qualifiers:
A
B
C
E
J
p
X
•
TIC is a possible aldol-condensation product resulting from sample extraction, (Organics)
Analyte also detected in the method blank.
Amendable Cyanide is a negative value due to an unknown interference.
Estimated concentration due to interference.
Estimated value below RDL or estimated value for TIC. (Organics)
Concentration difference between primary and confirmation columns > 25%. (Organics) The lower
result is reported. ·
Matrix interference which requires dilution or prevents the reporting of a result. Detection limits have
been adjusted where applicable.
Defined in report comments .
Solid samples (i.e. soil, sludge, and solid waste) are reported on a dry weight basis unless otherwise noted.
Test results relate only to the sample tested. Clients should be aware that a critical step in a chemical or
biological analysis is the collection of the sample. Unless the sample analyzed is truly representative of the
bulk of the material involved, the test results will be meaningless. If you have any questions regarding the
proper techniques of collecting samples, please contact us. However, we cannot be held responsible for
sample integrity unless sampling has been performed by a member of our staff.
WARRANTY AND LIMITATION OF LIABILITY -The accuracy of all analytical results is warranted for the
sample as it is received by the laboratory. Warranty for the integrity of the sample begins at the time it is
placed in the possession of authorized Davis & Floyd, Inc. Laboratories personnel. All other warranties,
expressed or implied, are disclaimed. Liability is limited to the cost of the analysis.
Davis & Floyd, Inc.
AD07_0/ (07/99)
000121
Davis & Floyd, Inc. j PO Drawer 428 j Greenwood, SC 29648 I Bl 6 E. Durst Avenue I Greenwood, SC 29649 j [phone] I Fax [phone]
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DATA ASSESSMENT CHECKLIST REPORT-LEVEL II
Client ID:
Project Number:
Monitoring Period:
Hoechst Celanese/Shelby
TFO26DB01
04/1999
Sample Delivery Group (SDG) Description:
Prepared By: Diane M. Rosseter
Date: · 12/9/99
Quarterly monitoring well samples collected and analyzed by Davis & Floyd, Inc. of Greenwood,
SC. 'The samples collected were analyzed for volatiles, ethylene glycol, and TOC according to EPA
SW-846 methodology.
CONTENTS LEVEL COMMENTS
II
Samole Results v All data Class A
Method Conformance Summary v O.K.
Chain(s) of Custody (COCs) v Various info incomplete. No
effect on data.
Master Tracking List v O.K.
Case Narrative
Samole Pren
Standards Preo
Instrument Qualitv Control Data
Batch Qualitv Control Reoort v O.K.
Surrogate Recoverv Report
Trio/Field/Equioment Blank Reoort v O.K. See note below.
Field Notes/Logbook v O.K.
CLP Forms
All Raw Data
Electronic Deliverables v O.K.
1) Samples collected 10/20/99 for ethylene gycol were not analyzed within holding time.
Replacement samples for ethylene gycol were collected on 11/9/99. No field notes were
taken for 11/9/99 sampling event.
Class A = quantitative Class B = qualitative Class C = unusable
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DAYIS
FLOYD
November 23, 1999
JERRY MCMURRAY
TICONA, LLC
P.O. BOX 87
SHELBY, NC 28151-0087
:L99102103
LABORATORY ANALYSIS REPORT
Login Number
Project Number
Description
: 60885. 00-0004
:GROUNDWATER SAMPLING & ANALYSIS
Dear Jerry Mcmurray:
We are pleased to provide the enclosed analytical results for the samples received by
Davis & Floyd, Inc. on October 21, 1999.
A formal Quality Assurance/Quality Control program is maintained by Davis & Floyd,
which is designed to meet or exceed the EPA or appropriate regulatory requirements.
All analytical analyses for this project met QA/QC criteria unless otherwise stated in the
footnotes. This report is to be reproduced only in full.
Feel free to contact our Client Services Representative at [phone] if further
explanation of the analysis is required. Unless other arrangements have been made, samples
will be disposed of or returned 14 days from the date of the report. We appreciate the
opportunity to provide services to your firm.
Sincerely,
DA VIS & FLOYD, INC.
~<//4.?
~. McCord, Jr.
Laboratory Manager
00,,0001 I Davi~ & F\oyd, Inc. I PO Drawer 428 \ Greenwood, SC 29648 I 816 E. l~urs1 Av'_enue I Greenwood, SC 2%49 I (B(>4) 229-4413 ) Fax [phone]
DAVIS
l~LfrYD LABORATORY ANALYSIS REPORT
Client
r;ont.act:
TICONA, LLC
P.O. BOX 87
SHELBY, NC 2B151-0087
JERRY MCMURRAY
Client ID: ITCI
Matrix
Parameter
Volatile Organicn
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETP..ACHLOROETHANE
1,1,2-TRICHLOROETHANE
1, l ·DICHLOROBTHANE
1,1-DICHLOROETl!ENE
1, 2-0ICJ-ILOROETHANE
1,2-DICHLOROPRQPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BBNZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CIILOROBENZENB
CHLOROETHANE
CHLOROFORM
CHLOROMETHANB
CIS-1,2-DICHLOROBTHBNE
CIS-1,3-DICHLOROPROPBNE
DIBROMOCHLOROMBTHANB
ETHYLBENZBNE
METHYLENE CHLORIDE:
NAPHTHALENE
STYRENE
TETRACHLOROETHBNE
TOLUENE
TRANS-1, 2-DICHLOROETHENB
TRANS-1, 3 -DICHI,OROPROPENE
TRICHLOROF.THENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
GW/ChemW
NC Certification Number: 25
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
Result
0.0050
0.00S0
0.0050
0.0050
0 .0050
0 .0050
0 .0050
0. 037
0.010
0.0050
0.20
0.026
0.0050
0.0050
0.010
0.012
0.0050
0. 010
0.010
0.0050
0.010
0.0050
0 .0050
0 .0050
0 .0050
0.0050
0.0050
0 .0050
0.0050
0 .0050
0.0050
0.0050
0.0050
0 .010
0 .010
0.0050
000002
Project Number: 60885.00-0004
Report Date November 23, 1999
Page 1 of 2
Sample ID L99102103-01
Date Collected: 2 0-OCT-9 9 12:15
Date Received 21-0CT-99
RDL Unito Analyst Date
0 .0050 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0 . 0050 mg/1 DSD 10/22/99
0 . 0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0.010 mg/1 DSD 10/22/99
0. 010 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0. 010 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0.010 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0.010 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0.010 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0.0050 rng/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0.0050 mg /1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0.0050 rng/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0 . 0050 rng/1 DSD 10/22/99
0.0050 mg/1 oso 10/22/99
0.0050 mg/1 oso 10/22/99
0. 0050 mg/1 DSD 10/22/99
0. 010 mg/1 DSD 10/22/99
0.010 mg/1 DSD 10/22/99
0.0050 rng/1 DSD 10/22/99
Time
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
1907
D;:ivis & floyd, lnc. I l'O Orav,•er 428 I Greenwood, SC 2%4H I 8 I(, L Durst Avenue I Greenwood, SC 29649 l (864) 229-441] ! fax [phone]
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DAVIS
FLtJYD LABORATORY ANALYSIS REPORT
client
Contact
TICOHA, LLC
P.O. BOX 87
SHELBY, NC 28151-0087
J8RRY MCMURRAY
Client ID: ITCI
P;1.rameter
Wet Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
NC Certification Number: 25
Project Number: 60885.00-0004
Report Date
Page 2 of 2
Sample ID
Result Qu;1,l RDL
November 23, 1999
L99102103-01
Units Analyst Date Time
1490 10.0 mg/1 TRB 10/28/99 1356
000003 I Davis & Floyd, Inc. I l'O Drawer 42B I Greenwood, SC 29()4B I 816 [. Durst Avenw.! I Greenwood, SC 2%4'J I (8fi4) 229-4413 I Fax [phone]
DAYIS
FI_j6YD LABORATORY ANALYSIS REPORT
Client
Contc1ct
TICDNA, LLC
P.O. BOX 87
SHELBY, NC 28151-0087
JERRY MCMURRAY
Client ID: ITCI DUP.
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1, 1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4 -METHYL-2-PBNTANONE
ACETONE
BENZBNE
BROMODICHLOROMETHANE
BROMOPORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROPORM
CH LOR OM ETHANE
CIS-1,2-0ICHLORORTHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZBNE
METHYLENE CHLORIDE
NAPHTHALENE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1, 3-DICHLOROPROPENE
TRICl!LOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
GW/ChemW
NC Certification Number: 25
<
<
<
<
<
<
<
<
<
<
Reault
0.0050
0.0050
0 .0050
0.0050
0 .0050
0.0050
0.0050
0.036
0.010
0 .0050
0.19
0.026
0.0050
0.0050
0.010
0.013
0.0050
0.010
0.010
0.0050
0. 010
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0 .0050
0 .0050
0 .0050
0.0050
0.0050
0. 010
0. 010
0.0050
000004
Project Number: 60885.00-0004
Report Date
Page 1 of 2
Sample ID
November 23, 1999
L99102103-02
Date Collected: 20-0CT-99 12:15
Date Received 21-0CT-99
Qual RDL Units Analyst Date
0 .0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0 .010 mg/1 DSD 10/22/99
0. 010 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0.010 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0 . 0050 mg/1 DSD 10/22/99
0.010 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0.010 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0.010 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0 . 0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0.010 mg/1 DSD 10/22/99
0.010 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
Time
1930
193 0
1930
193 0
1930
1930
1930
1930
1930
1930
1930
1930
1930
193 0
1930
193 0
1930
1930
1930
1930
193 0
1930
1930
1930
1930
1930
1930
1930
1930
1930
1930
1930
1930
193 0
193 0
1930
Davis & r:loyd, Inc. I 1'0 Drawer 428 I CrccnWo()d, SC 29(>4H I B 16 [. Ours1 Avenue I Greenwood, SC 2%49 I (B(,4) 229-441] I Fax (B(,4) 229-7119
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DAYIS
FLtlYD LABORATORY ANALYSIS REPORT
Parameter
Wet Chemistry
SW846 9060
Client
Contact
TICONA, LLC
P.O. BOX 87
SHELBY, NC 28151-0087
JERRY MCMURRAY
Client ID: ITCI DUP.
ORGANIC CARBON, TOTAL
NC Certification Number: 25
Project Number: 60885.00-0004
Report Date
Page 2 of 2
Sample ID
Result Qual RDL
November 23, 1999
L99102103-02
units Analyst Date Time
1480 10.0 mg/1 TRB 10/20/99 1418
000005 I Dav;s & Floyd, Inc. I 1'0 D,awe, 4211 I G,eenwood, SC 2%48 I 8 If, E. Du.st Avenue I G,eenwood, SC 2%49 I 18641 229-4413 I fax (8',4) 229-7119
I
LABORATORY ANALYSIS REPORT I
NC Certification Number: 25 I
Client TICONA, LLC Project Number: 60805.00-0004
P.O. oox 87 I
SHELBY, NC 28151-0087 Report Date November 23, 1999
Contact JERRY MCMURRAY Page 1 of 2 I Client ID: ITEF Sample ID L99102103-03
Date Collected: 20 OCT 99 12 : 40
Matrix GW/ChemW Date Received 21 OCT 99 I
Parameter Reault Qual RDL Unite Analyst Date Time
Volatile Organics
SW846 82GOB
1,1,1-TRICHLOROETHANE < 0.0050 0.0050 mg/1 DSD 10/22/99 1954
1,1,2,2-TETRACIJLOROETHANE < 0.0050 0.0050 mg/1 DSD 10/22/99 1954
1,1,2-TRICHLOROETHANE < 0.0050 0.0050 mg/1 DSC 10/22/99 1954
1,1-DIC!ILOROETl!ANE < 0.0050 0.0050 mg/1 DSD 10/22/99 1954 I
1,1-DICHLOROETHENE < 0.0050 0 .0050 mg/1 DSD 10/22/99 1954
1,2-DICHLOROETHANE < 0.0050 0.0050 mg/1 DSD 10/22/99 1954
1,2-DICHLOROPROPANE ' 0.0050 0.0050 mg/1 DSD 10/22/99 1954. I
2-BUTANONE < 0.010 0.010 mg/1 oso 10/22/99 1954.
2-HEXANONE < o. 010 0.010 mg/1 DSD 10/22/99 1954.
4.-METHYL-2-PENTANONE < 0.0050 0.0050 mg/1 DSD 10/22/99 1954.
ACETONE < 0. 010 0. 010 mg/1 DSD 10/22/99 1954. I
BENZENE ' 0.0050 0.0050 mg/1 DSD 10/22/99 1954
BROMODICHLOROMETHANE < 0.0050 0 .0050 mg/1 DSD 10/22/99 1954
BROMOFORM < 0 .0050 0.0050 mg/1 DSD 10/22/99 1954
BROMOMETHANE < 0. 010 0,010 mg/1 DSD 10/22/99 1954 I
CARBON DISULFIDE < 0.0050 0 .0050 mg/1 DSD 10/22/99 1954
CARBON TETRACHLORIDE < 0.0050 0.0050 mg/1 DSD 10/22/99 1954
CHLOROBENZENE < 0.0050 0.0050 mg/1 DSD 10/22/99 1954 I CHLOROETHANE < 0.010 0.010 mg/1 DSD 10/22/99 1954.
CHLOROFORM < 0.0050 0.0050 mg/1 DSD 10/22/99 1954
Cl!LOROMETHANE ' 0.010 0. 010 mg/1 DSD 10/22/99 1954.
CIS-1,2-DICHLOROETHENE < 0.0050 0.0050 mg/1 DSD 10/22/99 1954 I
CIS-1, 3-DICIILOROPROPENE < 0 . 0050 0 .0050 mg/1 DSD 10/22/99 1954
DIBROMOCHLOROMETHANE < 0 .0050 0 . 0050 mg/1 DSD 10/22/99 1954
ETHYLBENZENE < 0.0050 0 .0050 mg/1 DSD 10/22/99 1954
METHYLENE CHLORIDE < 0.0050 0.0050 mg/1 DSD 10/22/99 1954 I
NAPHTHALENE < 0.0050 0 .0050 mg/1 DSD 10/22/99 1954
STYRENE < 0 .0050 0 .0050 mg/1 DSD 10/22/99 1954
TETRACHLOROETHENE < 0.0050 0 .0050 mg/1 DSD 10/22/99 1954
TOLUENE < 0.0050 0 . 0050 mg/1 DSD 10/22/99 1954 I
TRANS-1,2-DICHLOROETHENE ' 0 .0050 0.0050 mg/1 DSD 10/22/99 1954
TRANS-1,3-DICHLOROPROPENB < 0.0050 0.0050 mg/1 DSD 10/22/99 1954
TRICHI,OROETHENE < 0.0050 0.0050 mg/1 DSD 10/22/99 1954 I
VINYL ACETATE < 0.010 0. 010 mg/1 DSD 10/22/99 1954
VINYL CHLORIDE < 0.010 0 .010 mg/1 DSD 10/22/99 1954
XYLENE (TCTAL) ' 0.0050 0.0050 mg/1 DSD 10/22/99 1954 I
000006 I
Davis & Floyd, Inc. I PO Dr;iwer 42B 1 Greemvood, SC 2964H I 81(> E. Durst Avenue I Greenwood, SC 29(J49 I {8(J4} 229-4413 I fJX (ll(>4) 229-7119 I
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DAVIS
FL6YD LABORATORY ANALYSIS REPORT
Parameter
Wet Chemiotry
SW846 9060
Client
Contact
TICONA, LLC
P.O. BOX 87
SHELBY, NC 28151-0087
JERRY MCMURRAY
Client ID: ITEF
ORGANIC CARBON, TOTAL
NC Certification Number: 25
Project Number: 60BB5.00-D004
Report Date
Page 2 of 2
Sample ID
Result Qual RDL
November 23, 1999
L99102103-03
Units Analyst Date Tiai.e
8.4 1.0 TRB 10/28/99 1437
000007
Davis & Floyd, Jnc. I PO Drawer 42B I Greenwood, SC 2964H I Hl 6 L Ours! Avenue I Greenwood, SC 2%49 I (fl(i4) 229-4413 I rax [phone]
DAVIS
FLtrYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA, LLC
P.O. BOX 87
SliELBY, NC 28151-0087
JERRY MCMURRAY
client ID: K-28
Parameter
Wet Chemiotry
SW846 9060
Matrix
ORGANIC CARBON, TOTAL
GW/ChemW
NC Certification Number: 25
Project Number: 60885.00-0004
Report Date November 23, 1999
Page 1 of 1
Sample ID L99102103-04
Date Collected: 20-0CT-99 14 :17
Date Received ' 21-0CT-99
Result ROL Units Analyet Date Time
183 1. 0 mg/1 TRB 10/28/99 1611
000008
Davis & Floyd, lnc. I PO Dr;iwer 4211 I Greenwood, SC 29fi48 I 8 l (J f:. Durst Avenue I Greenwood, SC 2%49 I (/1(,4) 229-4413 I Fax {llf>4) 2n-7119
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•1
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DAVIS
FLtJYD LABORATORY ANALYSIS REPORT
client
Contact
TICONA, LLC
P.O. BOX 87
SHELBY, NC 28151-0087
JERRY MCMURRAY
Client ID: V-23
Parameter
Wet Chemistry
SWB46 9060
Matrix
ORGANIC CARBON, TOTAL
GW/ChemW
NC Certification Number: 25
Result
Project Number: 60885.00-0004
Report Date
Page 1 of 1
Sample ID
November 23, 1999
L99102103-05
Date Collected; 20-0CT-99 15:15
Date Received 21-0CT-99
Qual RDL Unit.a Analyst Date Time
6930 20.0 mg/1 TRB 10/28/99 1544
000009
Davis & Floyd, Inc. I PO Drawer 428 \ Greenwood, SC 29648 I 81 (} [. Ours! Avenue I Greenwood, SC 29(i49 I (864) 229-441] ) Fax [phone]
DAYIS
FLt1YD LABORATORY ANALYSIS REPORT
client
Contact
TICOUA, LLC
P.O. BOX 87
SHELBY, NC 28151-0087
JERRY MCMURRAY
Client ID: TRIP BLANK
Mctt.rix
Parameter
Volatile organicn
SW84G 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1, 1, 2-TRIC!ILOROETHANE
1,1-DICHLOROETHANE
1, 1-DICHLOROETHENE
1, 2-DICHLOROHTHAtm
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOOICHLOROMETHANE
BROMOFORM
BROM OM ETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZBNE
CHLOROETHANE
CHLOROFORM
C!{LOROMET!IANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
M8THYLBNE CHLORIDE
NAPHTHALENE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLHNE (TOTAL)
GW/ChemW
NC Certification Number: 25
Project Number: 60885.00-0004
Report Date November 23, 1999
Page 1 of 1
Sample ID L99102103-06
Date Collected: 20-OCT-99 09: 00
Date Received 21-0CT-99
Result Qual ROL Units Analyst Date Time
< 0.0050 0. 0050 mg/1 DSD 10/22/99 2017
< 0.0050 0.0050 mg/1 DSD 10/22/99 2017
' 0.0050 0.0050 mg/1 DSD 10/22/99 2017
< 0.0050 0 .0050 mg/1 DSD 10/22/99 2017
< 0.0050 0 .0050 mg/1 DSD 10/22/99 2017
' 0.0050 0. 0050 mg/1 DSD 10/22/99 2017
' 0.0050 0 .0050 mg/1 DSD 10/22/99 2017
' 0 .010 0.010 mg/1 DSD 10/22/99 2017
' 0 .010 0.010 mg/1 DSD 10/22/99 2017
' 0.0050 0.0050 mg/1 DSD 10/22/99 2017
' 0.010 0.010 mg/1 DSD 10/22/99 2017
' 0 .0050 0 .0050 mg/1 DSD 10/22/99 2017
' 0.0050 0 .0050 mg/1 DSD 10/22/99 2017
' 0 .0050 0.0050 mg/1 OSD 10/22/99 2017
' 0. 010 0.010 mg/1 DSD 10/22/99 2017
' 0.0050 0.0050 mg/1 DSD 10/22/99 2017
' 0 .0050 0 .0050 mg/1 DSD 10/22/99 2017
' 0.0050 0 .0050 mg/1 DSD 10/22/99 2017
' 0.010 0.010 mg/1 DSD 10/22/99 2017
< 0.0050 0.0050 mg/1 DSD 10/22/99 2017
' 0.010 0. 010 mg/1 DSD 10/22/99 2017
' 0 .0050 0 .0050 mg/1 DSD 10/22/99 2017
' 0 .0050 0.0050 mg/1 DSD 10/22/99 2017
' 0. 0050 0. 0050 mg/1 DSD 10/22/99 2017
' 0.0050 0 .0050 mg/1 DSD 10/22/99 2017
' 0.0050 0.0050 mg/1 DSD 10/22/99 2017
' 0. 0050 0 .0050 mg/1 DSD 10/22/99 2017
' 0 . 0050 0.0050 mg/1 DSD 10/22/99 2017
' 0. 0050 o. 0050 mg/1 OSD 1.0/22/99 2017
' 0.0050 0.0050 mg/1 DSD 10/22/99 2017
' 0.0050 0 .0050 mg/1 DSD 10/22/99 2017
' 0.0050 0.0050 mg/1 DSD 10/22/99 2017
' 0 .0050 0.0050 mg/1 DSD 10/22/99 2017
' 0.010 0.010 mg/1 DSD 10/22/99 2017
' 0.010 0.010 mg/1 DSD 10/22/99 2 01 7
' 0.0050 0.0050 mg/1 DSO 10/22/99 2017
000010
0;1vis & Floyd, tnc. I PO Dr,1wer 428 I Greenwood, SC 29f>4B I 81 Ci E. Durst Avenue I Greenwood, SC 2%49 I (8(>4) 229-4413 I rax (B(,4) 229-7119
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DA,YIS
FLtiYD LABORATORY ANALYSIS REPORT
November 18, I 999
JERRY MCMURRAY
TICONA, LLC.
PO BOX 87
SHELBY, NC 2850
:L991 l 1005
:60885.00-0002
Login Number
Project Number
Description :GROUNDWATER SAMPLING & ANALYSIS
Dear Jerry Mcmurray:
We are pleased to provide the enclosed analytical results for the samples received by
Davis & Floyd, Inc. on November 10, 1999 .
A formal Quality Assurance/Quality Control program is maintained by Davis & Floyd,
which is designed to meet or exceed the EPA or appropriate regulatory requirements.
All analytical analyses for this project met QA/QC criteria unless otherwise stated in the
footnotes. This report is to be reproduced only in full.
Feel free to contact our Client Services Representative at [phone] if further
explanation of the analysis is required. Unless other arrangements have been made, samples
will be disposed of or returned 14 days from the date of the report. We appreciate the
opportunity to provide services to your firm.
Sincerely,
DAVJS ✓,;2
H. McCord, Jr.
ratory Manager
000011 I Davis & Floyd, Inc. I 1'0 Dnwcc 428 I Gccenwood, SC 2%48 I Bl 6 E. Dmsl Avenue I G,eenwood, SC 29649 I {HC,41 229-4413 I fax {8(,4) 229-7119
DAVIS
FI_Jt1YD
Client
Contact
TICONA, LLC.
PO BOX 87
SHBLBY, NC 2850
,JBRRY MCMURRAY
Client ID: ITCI
M<1trix
Parameter
Gas Chromatography
SW8'4G 8015
ETHYLENE GLYCOL
GW/ChemW
LABORATORY ANALYSIS REPORT
SC Certification Number: 241 JO
Project Number: 60885.00-0002
Report Date November 18, 1999
Page 1 of 1
Sample ID L99111005-0l
Date Collected: 09-NOV-99 11: 52
Date Received 10-NOV-99
Result Qual RDL Units Analyst Date Time
1040 70.0 mg/1 KLH 11/15/99 2123
000012
Davis & floyd, Inc. I PO Drawer 428 I Greenwood, SC 29(,411 I 81 G L Durst Avenue I Greenwood, SC 2%49 I (H64) 229-44 U I Fax (H64) 229-7119
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FLOYD
Client
Contact
TICONA, LLC.
PO BOX 87
SHELBY, NC 2850
JERRY MCMURRAY
Client ID: ITEF
Matrix
Parameter
Gae Chromatography
SW846 8015
ETHYLENE GLYCOL
GW/ChemW
LABORATORY ANALYSIS REPORT
SC Certification Number: 241 JO
Project Number: 60885.00-0002
Report Date November 18, H99
Page 1 of 1
Sample ID L99111005-02
Date Collected: 09-NOV-99 11 :49
Date Received 10-NOV-99
Result Qual RDL Units Analyst Date Time
< 7.0 7.0 mg/1 KLH 11/15/99 1931
000013
Davis & Floyd, Inc. I PO Dr,iwer 42B I Greenwood, SC 2%48 I 816 [. Durst Avenue I Greenwood, SC 29(,49 I (8G4) 221J-4413 ) Fax (B64) 229-7119
Client
Contact
TICONA, LLC.
PO BOX 87
.SHELBY, NC 2850
,JBRRY MCMURRAY
Client: ID: ITEF DUP.
Matrix
Parameter
Gaa Chromatography
SW846 8015
ETHYLENE GLYCOL
GW/ChemW
LABORATORY ANALYSIS R.EPORT
SC Certification Number: 24110
Project Number: 60885.00-0002
Report Date November 18, 1999
Page l of 1
sample 1D L99111005-0J
Date Collected: 09-NOV-99 11 : 49
Date Received 10-NOV-99
Qual RDL Onita Analyst Date Time
< 7.0 7.0 mg/1 KLH 11/15/99 2055
000014
Davis & Floyd, Inc. I PO Drawer 4213 I Greenwood, SC 2%48 I Hl b L Dur'.>\ Avenue I Greenwoo<l, SC 29649 I (8fi4) 229-4413 I r:ax [phone]
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I FLOYD
Engineering
Architecture
Environmental & Laboratory Services
I, PO. Drawer 428
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Greenwood, SC 29648 • 816 East Durst Avenue Greenwood, SC 29649 • [phone] (office) [phone] (fax)
Method Conformance Summary
Client: HNA HOLDINGS, INC.
Log;n, L99102103
Criteria Volatiles
Sample Holding Time
Standards Preparation
Instrument Tuning
Instrument Calibration
Calibration Verification
Deeradation Check
Interference
Sample/Standard
Blanks Results
Method Accuracy
Method Precision
Surrogate Recovery
PDS/SD/MSA
TCLP Preparation
Key ✓
NIA
Met Criteria Met
Not Applicable
✓
✓
✓
✓
NIA
NIA
✓
✓
✓
✓
NIA
NIA
Semi
Volatiles Metals
NIA NIA
NIA NIA
NIA NIA
NIA NIA
NIA NIA
NIA NIA
NIA NIA
NIA NIA
NIA NIA
NIA NIA
NIA NIA
NIA NIA
NIA NIA
*
PDS -
SD -
MSA-
Method Criteria Not Met -See footnote(s) below.
Post Digestion Spike
Serial Dilution
Method of Standard Additions
Footnotes: TOC is summarized under "Inorganics" column.
Ethylene glycol is summarized under "Other" column.
Project Number: 60885.00-0004
Report Date: November 23, 1999
Inonrnnics Other
✓ 1
✓
NIA NIA
✓ ✓
✓ ✓
NIA NIA
NIA NIA
✓ ✓
✓ ✓
✓ ✓
NIA NIA
NIA NIA
NIA NIA
1 The original analyses of ethylene glycol exceeded the 7-day holding time by 1 day.
Samples were recollected and reanalyzed within the holding time. The second
analysis is reported.
Preparedbo+ DL
000015
DAVIS
l~Li5YD LABORATORY ANALYSIS REPORT
Master Tracking List
client
Contact
Sample ID
L99102103-01
Volatile Organics
SW846 8260B
Wet Chemistry
SW846 9060
L99102103-02
Volatile Organics
SW846 826GB
Wet Chemistry
SW846 9060
L99102103-03
Volatile Organics
SW846 8260B
Wet Chemistry
SW846 9060
L99102103-04
Wat Chem.iBtry
SW846 90GO
L99l02103-05
WE!t Chem.iBtry
SW846 9060
L99102103-06
Volatile Organics
SW846 8260B
TICONA, LLC
P.O. BOX 87
SHELBY, NC 28151-0087
,JERRY MCMURRAY
Client ID
ITCI
ITCI DUP.
ITEF
K-28
V-23
TRIP BLANK
NC Certification Number: 25
Project Number: 60885.00-0004
Report Date
Page 1 of 1
November 23, 1999
Date Collected Date Received
20-0CT-99 12:15 21-OCT-99
10/22/99 1907
10/28/99 1356
20-0CT-99 12:15 21-OCT-99
10/22/99 1930
10/28/99 1418
20-OCT-99 12:40 21-OCT-99
10/22/99 1954
10/28/99 1437
20-0CT-99 14:17 21-0CT-99
10/28/99 1611
21-0CT-99
10/28/99 1544
20-0CT-99 09:00 21-0CT-99
10/22/99 2017
000016
D,ivis & rloyd, Inc. I 1'0 Drawer 42B I Greenwood, SC 2%4H I B 1 fJ t. Durst Avenue I Greenwood, SC 2%49 I (B64} 229-44 JJ I rax (M,4) 229-7119
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FLOYD LABORATORY ANALYSIS REPORT
Master Tracking List
Client
Contact
Sample IO
L99111005-01
Gas Chromatography
SW846 8015
L99111005-02
Gas Chromatography
SW846 8015
L99111005-03
Gas Chromatography
SW846 8015
TICONA, LLC.
PO BOX 87
SHELBY, NC 2850
JERRY MCMURRAY
client ID
ITCI
ITEF
ITEF DUP.
SC Certification Number: 241 JO
Project Number: 60885.00-0002
Report Date
Page 1 of 1
November 18, 1999
Date Collected Date Received
09-NOV-99 11:52 10-NOV-99
11/15/99 2123
11/15/99 1931
09-NOV-99 11:49 10-NOV-99
11/15/99 2055
000017
D,wis & Floyd, Inc. I PO Drziwer 428 I Greenwood, SC 29(>48 I 81(1 f.. Durst Avenue I Grl'enwood, SC 2%49 I (8(,4) 229-441] I fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Surrogates % Recovery
· Measu·reDate
L99102103-0l
L99102103-02
L99102103-03
L99102103-06
LCS19380:1
MB193B0:1
MS99102107-09:19380
MSD99102107-09:19380
22-0CT-99
22-OCT-99
22-OCT-99
22-0CT-99
22-0CT-99
22-0CT-99
22-OCT-99
22-0CT-99
DCE
BFB
TOL
1,2-DICHLOROETHANE-D4
BROMOFLUOROBENZENE
TOLUENE-DB
19 : 07
19: 30
19 : 54
20 :17
22 :39
16:22
21: 05
21 : 28
98 .4 95.8
97.8 95 . '
99.2 95.4
102. 4 96.2
104.1 94.4
99.6 93.3
114.7 96.6
1l5 .5 96.8
Report Date
Page 1 of 1
Matrix
Method
95.7
95.7
96.1
95.2
96.1
96 • 0
92 .8
92.2
000018
November 01, 1999
GW/ChemW
SW846 8260
Davis & floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue l Greenwood, SC 29649 J (U(>4) 229-4413 j fax (B64) 229-7119
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FLOYD
Method Blanks
Blank
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BCITANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TBTRACHLORIDE
CHLOROBHNZBNE
CHL0R0ETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
NAPHTHALENE
STYRBNB
TETRACHLOROETllENE
TOLUBNE
TRANS-1,2-DICHLOROETHENE
TRANS-1, 3 -DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDB
XYLENE (TOTAL)
MB193BO:l
LABORATORY ANALYSIS REPORT
Cone
< 0.0050
< 0.0050
< 0.0050
< 0 .0050
< 0.0050
< 0.0050
0.0050
< 0. 010
< 0. 010
< 0.0050
< 0. 010
< 0.0050
< 0.0050
< 0.0050
< 0. 010
< 0.0050
< 0.0050
< 0.0050
< 0.010
< 0.0050
< 0. 010
< 0.0050
< 0 . 0050
< 0 .0050
< 0.0050
< 0.0050
< 0. 0050
< 0.0050
< 0.0050
< 0 .0050
< 0.0050
< 0 .0050
< 0.0050
< 0.010
< 0 .010
< 0.0050
00001'9
Report Date
Page 1 of 1
November 02, 1999
Matrix GW/ChemW
WorkGroup: WG193BO
RDL Onita Analyst Date
0 .0050 mg/1 DSC 10/22/99
0.0050 mg/1 DSC 10/22/99
0 .0050 mg/1 DSD 10/22/99
o. 0050 mg/1 DSC 10/22/99
0. 0050 mg/1 DSD 10/22/99
0. 0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSC 10/22/99
0.010 mg/1 DSD 10/22/99
0.010 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0.010 mg/1 DSD 10/22/99
0.0050 mg/1 DSC 10/22/99
0. 0050 mg/1 DSC 10/22/99
0. 0050 mg/1 DSD 10/22/99
0.010 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0. 0050 mg/1 DSC 10/22/99
o. 0050 mg/1 DSD 10/22/99
0.010 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0.010 mg/1 DSD 10/22/99
0. 0050 mg/1 DSC 10/22/99
0.0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSC 10/22/99
0.0050 mg/1 DSC 10/22/99
0.0050 mg/1 DSC 10/22/99
0.0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0.0050 mg/1 DSD 10/22/99
0 .0050 mg/1 DSD 10/22/99
0.010 mg/1 DSC 10/22/99
0 .010 mg/1 DSC 10/22/99
0.0050 mg/1 DSC 10/22/99
Time
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
1622
I Dav;s & Floyd, Inc. I PO Drawcr428 I Greenwood, SC 2%48 I 81r, [. Durst Avenue I Greenwood, SC 2%49 I (8(,4) 229-4413 I Fax [phone]
DAYIS
FLbYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
M.'3/M.SD
Parameter
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
Pa·r~met~r
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENB
TOLUENE
TRICHLOROETHENE
MS99102107-09:193BO
MS099102107-09:19380
Report Date
Page 1 of 1
November 01, 1999
Matrix GW/ChemW
WorkGroup: WG193Bo·
Method SWB46 8260B
.sPik:C\, \:?i:'V~~-~Pie':': lf::f.:/MS :;:
~~d-~./ .·-.-·::\c6~:~{\?··· /:~~~\ ··.
M·S:i./'
:}1R_E~·
120.7
104.8
101.S
99.7
105.2
.·.-r..i,i't"~ ::-: :-•:.-
\"Ri:c/'"
50.00
50.00
so. 00
so. 00
50. 00
50.00
50.00
50.00
50.00
50.00
< 5. 00
< 5.00
< 5.00
< 5.00
< 5. co
59.95
52. 53
51. 43
49.83
53 . 3 2
000020
60.33
52.41
50.74
49.86
52.59
119.9
105.
102.9
99.7
106. 6
0.632
0. 22 9
l. 35
0.0602
. 38
74-130
89-120
89-115
86-120
86-122
9
10
' 7
12
74-130
89-120
89-115
86-120
86-122
Davis & rloyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (B64) 229-4413 I F.ix (B(J4) 229-7119
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DAYIS
FLbYD LABORATORY ANALYSIS REPORT
LaboraJory Control Standards and DuplicaJes
LCS
::-:/~~rameter
1,1-DICHLOROETHENE
BENZENE:
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
LCS19380:l
: SI\k~}k
·Adaea{:
20.00
20 00
20.00
20.00
20. 00
21. 50
20.33
20.08
20 27
20. 24
Report Date
Page 1 of 1
November 01, 1999
Matrix GW/ChemW
WorkGroup: WG19380
Method
107.5
101. 7
100.4
101. -4
101.2
SW846 8260B
74-12S
90-119
B9-116
87-120
86-120
000021 I Dav;s & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2%48 I 81(, E. Durst Avenue I Greenwood, SC 2%4'l I {1164) 229-4413 I Fax {864) 229-7119
DAYIS
Fl1tlYD
Method Blanks
Parameter
Wet Chemistry
SW846 !}060
Blank
ORGANIC CARBON, TOTAL
MB19439:1
LABORATORY ANALYSIS REPORT
Report Date
Page 1 of 1
Matrix
November 01, 1999
GW/ChemW
WorkGroup: WG19439
Cone: Qual RDL Uni ta Analyst Date Time
1.0 1.0 TRB 10/28/99 1725
000022
Davis & Floyd, Inc. I PO Drawer 4211 I Greenwood, SC 29648 I 816 E. Dur'.:>1 Avenue I Greenwood, SC 2%49 I {ll64) 229-4413 I r-ax [phone]
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DA,YIS
FLtlYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
·.··Parameter
ORGANIC CARBON, TOTAL
-_:Pari:tmeter
ORGANIC CARBON, TOTAL
HS99102104-04:19439
MSD99102104-04:19439
Report Date
Page 1 of l
November 01, 1999
Matrix GW/ChemW
WorkGroup: WG19439
Method SW846 9060
·sPi_~~ _-:·· \::#·~;;~-.r·=· ··-:·Ms·:-
Ad;i;d.,-,·-.. :+\C6h~'.(: ... . co~c
. -·MS
. ·-· :-:.,·R~d
. L·ictlits· ...
·=·--,/~k~}'❖ •
20. 00 B.BS 28.60
20.00 2 B. 10 96.3
000023
98.8
·.-·::=\RPD
1. 76
77-121
17 77-121
I Dav;s&Floyd,lnc. I POD,awec428 I G,ccnwood,SC2964!l I 816E.Ducs1Avenue I G,eenwood,SC29649 I [phone] I Fax[phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS LCS19439:1
·Parameter
ORGANIC CARBON, TOTAL 10.00 10.30
Report Date
Page 1 of 1
Matrix
November 01, 1999
GW/ChemW
WorkGroup: WG19439
Method SW846 9060
103.0 90-110
000024
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Method Blanks
Blank
Pa.ra.meter
Gas chromatography
SW846 8015
ETHYLENE GLYCOL
MB19658:1
LABORATORY ANALYSIS REPORT
Cone
7.0
000025
Report Date
Page 1 of 1
Matrix
November 18, 1999
GW/ChemW
WorkGroup: WG19658
Qual RDL Units Analyst Date Time
7.0 KLH 11/15/99 1806
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 2%48 I HH, E. Durst Avenue I Greenwood, SC 29649 I (864) 229·4413 I Fax [phone]
DAVIS
FI-1tiYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
ETHYLENE GLYCOL
(;~'~a~e_i:er
BTHYLENE GLYCOL
MS99111005-02:19658
MSD99111005-02:19658
Report Date
Pagel of
Matrix
November 18, 1999
GW/ChemW
WorkGroup: WG19658
Method i>WB46 8015
:S"i:ii_k_t;'-; .. :·-:\/=B~:;i~{f ,:,.;:?H"S)'C:=·
'Ada·~·d·;:::::,::•:,.· ·c6~~/( :.'(Ji~}'
.. , ·=··:)\/H~t·
.,',:~1u,:c. · IRBC
73-116 50.00 8.67 53.32 89.4
., .
.. :·_··:;_l/,iPo:.: Liiniti:i
::tRP~ :·. •0 ~-· ·• ·
50.00 52.63 87.9 1. 38 20 73-116
000026
Davis & Floyd, Inc I PO Drawer 42B I Greenwood, SC 2<J64B I 816 l:. Dur'.:>l Avenue I Greenwood, SC 2%49 I (IH>4} 229-441 J I F,1x [phone]
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DAIIS
FLOYD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
· · ·P?rameter
ETHYLENE GLYCOL
LCS LCSl.9658:1
50.00
Report Date November 18, 1999
Page l of 1
Matrix GW/ChemW
WorkGroup: WGl.965B
Method SW846 8015
47.19 96.1 64-117
000027 I Dc0vis & Floyd, Inc. I 1'0 Dcawe, 428 I Gceenwood, SC 2%48 I 81(, [. Du,st Avenue I Gceenwood, SC 2%49 I 181,4) 229-441J I Fax (8&41229-7119
.. --
Client
Ticona
Shelbv,NC
Contact
Jeff Randoloh
Collected By
J.G. Jenkins, If/
NOTICE:
Sample Oescriotion
Trin Blank
I TC -r
'Ti(,.,.
m
no,Ceived ByQ •
---
Project I Sile Location
60885.00, Task 0004
Report To
Samole Collection
Date Time
/ot,Jttl na~-
11.1,
12..I C:
l'V-10
114 ll
Date Time Reliquished By
,./,,1,, 0~
Date Time Received By
- -
Copy To
.. ~ • " Time
'x 5
'I. 5
X 5
)( 5
'{ 5
i 5
---- ---Chain of Custody Record
816 E. OurstAvenue, Greenwood, SC 29649 [phone] Fax: [phone]
Laborato,y Cenifca/ion Numbers· SC-24110, NC. 25, TN -2923, VA-77
Reporting Requirements: { J Stanctard { J Data Package (Specify Level)
Required Parameters, Containers and Prese,vatives
" ~ E " -~ E E ~ :<1 " ~1 0 -" N
e m 0 0 .s iEi
%
~ ~ " 8 ~ ~ f'. £ 0 V " " " V ' " e; C h. D V E u ~ ~, , ~ 0 £ z ~ w
Total C B A ,.;
1.. ?_ '\'
~ 'L. I ,,{ ~Ye
C: '2..... I ;,{ /\'
C: 2. I / \ \
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Date Time Reliquished By Date Time
Date Time Date Time
---..
State
NC
L.0!-lln
"" 0
j ~ -e g ~ ~ . ,.~
Cb • • . ,; -. . ~ .~ ><
..J R ~
Fraction HOT
th
01
r, 2
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a5
Page _l_ of .l__
.., .. ice use Univ
Purchase Order
Ouo/e
Special Instructions
vommen1s
oc
C\.I
C
C
0
0
tJ }00
Icommen/s
Matrix Type Definitions
Preservative Definitions
1 -Drinking Water 2 • Clean Water 5 -Groundwater 7 · Soil/Sediment 8 • Liquid Sludge 9 -Oil 12 · Air
A -None B • H2S04 C • HCI D -HNO3 E -NaOH F -Filtered G • Other
Cooler ID~ailable): /
On Ice: ~I No T-,-m~p(-C-1---., -2..,..c,,if,:---
Custody Seal: Intact / Broken / NonJ
Davis & Floya, Inc.
FL02_01 (02199)
D~IS"'""'"' ~ J.rdlitfnlr~ FL YD hrttomesu.l &i Lffl&1.iry 8micea
Client Project I Site Location
TICONA 60885.00/T0002
Shelbv,NC
Contact Report To Copy To
Johnnv Ledford
Collected By
John McMahan
NOTICE:
? go :; a 0 0 E .~ l :}! -g 8.
~ ~ EP~ !§ E Samole Collection i= :~ ~ 8 e (!) :,
Sample Descriotion Date Time Time Tvne
ITCI JU -'i< I /,;("?II :,( 5
ITEF // ljq X 5
ITEF Duo \ / II ~ ~ ;( 5
/ '
Reliquished ~!di;? Date Time Reliquished By
/,J //-1,-11 ,;.fee
?ledB
. Dale Time Received By
I Comments
A){) _.f,.r5, C,/ f fi./?'J,,f"1/T'
Chain of Custody Record
818 E. Durst Avenue, Greenwood, SC 29649 [phone] Fax: [phone]
Laboratory Certifcation Numbers: SC-24110, NC-25, TN-2923, VA-77
Reporting Requirements: { } Standard [ J Data Package (Specify Level)
Required Parameters, Containers and Preservatives
(!)
E ls
" ·! 13 0 ~ u
0 (!)
.!l 0 C • E "' a £ z w
Total A
"2'. l
i! 7
"-~
Date Time Reliquished By Date Time
Date Time Received in Lal:>orat~y , Date Time
ft5A (ft. /h',s 1/.10.[la Otoo
Page-.J--of _f_
vu/Ce use vmy
Purchase Order
State Quote
NC
tomn Special Instructions
5
J ~~ 0 • C N ~ . ,., ~
C "0
:i'.: f3 -· ~~ ...J .s
Fraction HOT ommems
01
({)~
03
Ouickc Shipg
y N ~-CUENT
"" FEDE>:
If :,:;ecify: Airbi/1 Number
__ days
Coolec l~ble)c /
On Ice: Yes o Temp(C)n~
Custody Seal: Intact / Broken Non
er.
N
0
0
0
0
Matrix Type Definitions 1 -Drinking Water 2 • Clean Water 5 • Groundwater 7 -SoiVSediment 8 • Liquid Sludge g.m 12-Air Davis & F,oyu, Inc.
Preservative Definitions A -None B • H2S04 C -HCI D -HNO3 E -NaOH F -Filtered G • Other FL02 _01 (02199} ------.. ---111111 ---.. -- --
Df\YIS
FLffi'D
ENGIN(CRS
PLANN(RS
ARCHIT(CTS
SCIO-HISTS
FIELD DAT A LOG
,D~l;c.i,
~//,ct~
CHARLESTON • GREENWOOD '" COLUMBIA
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
Well No· ITCI.. ..
Clicnl: T;~~~· s reefs} o{L\~)\fO.blt 10 Lobel (yes/no)
Sile Nome: S~e\L A1L Job No.: (O:l<f;5".oO Well C plelion: Proleclive Cosing (yes/no) flush (yes/no) ,;
Oafc: wl-i.oh~ LWR submilled by: -flush-Moun over Seal lnlacl (yes/ n~) locking Cop {yes/no)
Sampling Personnel: "S-G. :S-enk,ls :m Locked al Arrivo es/no) Deporlure (yes/no) '
Site Personnel: AJn"'· Well Cosing (height a ve/deplh below) ground: fl.
Regulatory Personnel: /VO "8 Cosing Type (PVC) (Steel) her)
Weather Conditions: Arrt:w, llfll!.i~~I S kifllll~ Temp.: 6 0 Dedicated Pump or Boiler (yes o) Type
Well Oiameler: A I {_A-In. Proleclive Post/ Abutment (yes/ no) ncrele Pod (yes/no) -~
(A) Top of Well Elevation: \ msl (yes/no) Well Integrity Solisfoclory (yes/no) If no, e loin below.
(B) Depth to Immiscible Loyer: ' Well Yield. ( low / moderate / high ) f I.
(C) Immiscible layer Elevolion: (A)-(1 = msl {yes/no)
(0) Depth lo Groundwater. fl. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(0)= ms! (yes/no) DIA. or PiPE (in.) VOLUME IN GAL/rt.
1.0 0.041
(r) Tola! Well Depth = It. 2.0 0.163
3.0 0.367 (G) length of Waler Column: (r)-(0)= It. 4.0 0.653
5.0 1.020 Cosing. Volume = (G) x Volume in got./1~ ools. 6.0 1.470
Method of Well Evocuolion Start Time: TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOVE FIGURES BY
6:(ah I t i.S-3.8 LITERS/GALLON. Melhod of Sample Colleclion Time:
Chain-of-Custody r orm Storied @no)
.
FIELD ANALYSES s,.fk D~lic44e
1st Volume 2nd Volume 3rd Volumo Hh \£elt::1me 6th Yeltfffte.
Volume Purged (gallons) --Time (mililory) I 1. IS-t 7. tr
pH (S.U.) !;. I -s. Sp. Cond. (umhos/cm) I 77 I I -,.., ...,
Waler Temp. ("C) 'I q • I ' -.,
Odor (subjcclive)• II J.l
Turbidity {subjeclive)" r ' • (t)None (2)Slighl (3)Moderole ( 4)Slrong
" (t)Cleor (2)Stighlly Turbid (3)Moderalely Turbid (~)Very forbid (5)Exlremely Turbid
Commcnts/Obscrvotions/Recommendatians: AJfA"-Ab+ A pp) :,a},\,
FORM COMPLETED BY: ~-: ~ , ill
0A1E, 1£>l-zol ~ ""''
O& r form48 (3/94)
000030
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D1\)/1S
I FL6YD
(NCIN[[RS
PLANNERS
ARCHITECTS
SCIOHISTS
FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS CHARLESTON • GREENWOOD • COLUMBIA
I Clienl:_J_l.L(;ln:~--------------
Well No.: JTf p
!Jct AtY1 i e Source(s) of1'11el D ________ ID Label (yes/no)
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Sile Name: ..,5.,_~'-""\__.,h~,1-, .....v,A.JL[k._ ___ Job No.: ~O8:t,[. 0Q
0ale: ,olwl~, LWR submillcd by:_-_____ _
Sampling Personnel: __ 3...,,_ • ...,C.c.;·:....__::S,.,1uo.l.!I'-'< 1u' \c,( _ _.,_,m ... 1.-~---
Sile Personnel: ___ /_lLf.l..'ll\_t,_ _________ _
Regulatory Personnel:._...J.lA
0
,.1.l..sO'-"C\stl __________ _
Weolher Condilions:Ovuu~4, Ol14<;0'◄1 s1,wn Temp.: b D
Well Diomeler: f.,J f A: In.
Well C plelion: Proleclive Cosing (yes/no) Flush (yes/no)
Flush-Mounl over Seal lnlacl (yes/no) Locking Cop (yes/no)
Locked al Arrival s/no) Departure (yes/no)
Well Cosing (heigh! abo /deplh below) ground: ______ _1f1,_I.
Casing Type (PVC) (Sleel) ( er) ___________ _
0edicoled Pump or Boiler (yes/n Type
Proleclive Posl/Abulmenl (yes/no) C crele Pad (yes/no)
(A) Top of Well £1evolion: _..__ _______ msl (yes/no) Well lnlcgrily Solisfaclory (yes/no) If no, ex in below.
(Bf Oeplh lo Immiscible Layer: fl. Well Yield. ( low / moderale / high )
(C) Immiscible Layer [levalion: ( msl (yes/no)
(D) 0eplh lo Graundwaler. fl.
(E) Graundwoler Elevolion: (A)-(0)= ,.__ _____ msl (yes/no)
(F) Tolal Well 0eplh = fl.
(G) Lenglh af Waler Column: (F)-(0)= fl.
Casing Volume ::: (G) x Volume in goL ols.
Mefhod of Well Evacuation ------l'--Slart Time: ___ _
Method of Sample Colleclion -----'\,1-L.Jd.JJ-___ Time: \ 'V::\ 0
Choin-of-Cuslody Farm Slarted
WELL VOLUME 0ATA
0IA. OF PIPE (in.) VOLUME IN GAL/Fl.
1.0
2.0
3.0
4.0
5.0
6.0
0.041
0.163
0.367
0.653
1.02D
U70
TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOVE FIGURES BY
3.8 LITERS/GALLON.
::===============================---===============================:
Volume Purged (gallons)
Time ( mililory)
pH (S.U.)
Sp. Cond. (umhos/cm)
Waler Temp. ("C)
Odor (subjeclive)•
Turbidily (subjeclive)"
1st Volumo
.
FIELD ANALYSES
2nd Volume 3rd Volume 4th Volume -'l,1\1) ..
-~ "' 'G._ 8. 1.
" ~,,/'\
l'l
?..
I
' (l)None (2)Slighl (3)Moderole (4)Slrong
, .__"_(!.:1.!..)C:..:le:..:a:..:r-'-(2:!.):..:Sl'-=ig:..:hl21y_T:..:u:..:rt,:..:id:._~(3.!..)M:..:o::d:..:er::ol::el.!..y:..:T::urt,=id~(:..:~)..:_V:::ery!...:..:r:::ur::b:.::id~(::_5)'.:E:..:xl:..:re::.:m::e:;_IY_:T::_urn:.::.::id~--------------_i
Commenls/Observolions/Recommendolions: A 1/A : ,\ lat flwl•, C• hie Alo Iola\ Res:dlA I c,hb:; Oe J,:t,,~
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FORM COMPLETED BY: &,?S. tr~ IK
0ATE: -~lo'L}--'-fJ\,/clc__JTu"l""L-' _' __
D& F f orm48 (3/94)
000031
Df\YIS
FLOYD
[NCINECRS ARCHITECTS
PLANHCRS SC!CHT1S1S
FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS CHARLESTON • GRCENWOOO '" COLUMBIA
Well No · ~ • c.. ~ ..
~
Source(s) of Well ID k:: • 7 ~) /vlol'.l ID Lobel 9-'no) Client: I I l OD"'
Sile Name: Sliill., l/C Job No.: 6C11i:ll:• O(l Well Complelion: Prolcclive Cosing ~no) rlush (yes@ .,
Flush-Moun! Cover Seal lntocl fre(to) locking Cap Ms no) Dole: JOh,o/ 9<\ LWR submilled by: -
Sampling Personnel: 3-G. ::S,.,l<;nI , [jJ_ Locked ol Arrival eno) Oeporlure (Gv'no)
Sile Personnel: I\ J. "' Well Cosing (heighl obove/deplh below) ground:~
Regulatory Personnel: A II),-,, Cosing Type (PVC) B (Of her)
Weal her Conditions: 01tc c, aQ I D lltJ.S, QoA ~ ,.),,..,16 Temp.: bO Oedicoled Pump or Boiler £no) Type fi\.U,c
Well Oiamcler: l.-o In. Proleclive ~bulmenl es no} Concrele Pod (E3/no)
(A) Top of Well Elevolion: ~ 11, l..0 msl (yes/no) Well Integrity Salisfaclory @,'no) If no, explain below.
(B) Depth to Immiscible Loyer. -f I. Well Yield. G/ moderofe / high ) S,e N•i,
(C) Immiscible Loyer Elevotion: (A)-(B)= -msl (yes/no)
(0) Depth to Groundwoter. "LQ-s <-ft. WELL VOLUME DATA
(E) Groundwofer [levotion: (A)-(0)= 7 ,o. 68 msl (yes/no) DIA. or PiPE (in.) VOLUME IN GAL/rt.
1.0 0.0◄1
(F) Toto! Well Oeplh = l.~ -~ ft. 2.0 0.163
3.0 0.367 (G) Length of Wofer Column: (r)-(D)= 7, Lj~ ft. ◄.O 0.653
I, L 5.0 1.020 Cosing Volume = (G) x Volume in goi./fi.= gals. 6.0 1.◄70
Mefhod of Well (vocuafion PL!~ Start Time: ) l:l l...J ~ TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOVE rlGURES BY
Y.,--11:l 17
3.8 LITERS/GALLON. Method of Sample Collecfion Time:
Chain-of-Custody f" orm Started {isjto)
FIELD ANALYSES
1st Volume
Volume Purged (gollons) I, 1..
Time (military) I ", S-=l
pH (S.U.) l.l-
Sp. Cond. (umhos/cm) q ('.)
Wofer Temp. (•c) I
Odor (s.ubjective)• I
Turbidity (subjecfive)" ·. "L
• (!)None (2)Slighl (3)Moderole (◄)Strong
" (1 )Cleor (2)Slightly Turbid (3)Moderofely Turbid
Comrnenls/Observo1:ons/Recommendolions: lffA :
lit L 1tnlv"'" ij),lfy,\ q;,i,i,1,ly
\10!1Jme {oolt. l<Jo1d, rJI., lo"¥,•'·
2nd Volume 3rd Volume
l,. 4 3,..,
... ,-'l It..\\ y
i,. t. (,, , (,
~ , q, l.O I~
~ ,e
1-1 'i
I I
(◄)Very Turbid (5)Extremely Turbid
A~h /)It,\,
cnlvr..r,
M
dr«ld••
000032
4th Volume
To!.I jki t~I
do,.,. si,cl
-
5th Volume.
D& r form48 (3/9◄)
fl.
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I D1')/1S
I FLOYD
ENGINEERS
PlANHCRS
ARCHITECTS
SCl[tHISTS
FIELD DAT A LOG
FOR GROUNDW A TEA SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
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CHARLESTON • GREENWOOD • COLUMBIA Well No· V-c3 ..
Clienf: 1, C n n. Source(,) of Well 10 Map · 10 lobel®/no)
Sile Nome: .Sh! I ~,11 t:,1 l. Job No.: ~ 0 8-Fi ,\. 0 Q Well Complefion: Proleclive C,,sing e/no) flush (yes~
Dale: /ol?,O I 1 ~ ' M:1 . p, LWR submilled by: -Flush-Moun! Cover Seal lnfacf ~es/no) locking Cop (yes no)
Sampling Personnel: -:s-. C,. -:S-f ol<;,1, llI locked of Arrival ~/no) Oeporlure @no)
Sile Personnel: N12"'· Well Casing (heigh! above/depfh below) ground: 3
Regulatory Personnel: Aln"~ Cosing Type {PVC) (~) (Ofher)
Weather Conditions:Ovcrt,td I O(Wi0!11I S b~I.~~,,~ Temp.: {;O Dedicated Pump or Boiler ~/no) Type EJ.H.1.,
Well Diameter: L-0 In. Protective Post/Abutment (yes,€g} Concrete Pod ~no)
(A) Top of Well Elevafion: 8:11-1-~ msl (yes/no) Well lnfegrily Safisfacfory ~/no) If no, explain below.
(B) Oepfh fa Immiscible layer. -ff. Well Yield @; moderate / high ) 5 « /vo1e
{C) Immiscible layer Elevafion: (A)-(B)= -msl (yes/no)
(0) Depfh lo Groundwofer. I fi. s1 ff. WELL VOLUME DATA
{E) Groundwofer Elevation: (A)-(D)= 71H, l'L msl (yes/no) DIA. or PIPE (in,) VOLUME IN GAL/ff.
t.0 0,041
(F) Tofal Well Depth = 'l...? -~ ff. 2.0 0.163 ~. ~~ 3.0 0.367 (G) lenglh of Waler Column: (f)-(D)= fl. 4.0 0.653 ,., 5.0 t.020 Casing Volume = (G) x Volume in gal/fl.= gols. 6.0 1.470
Method of Well Evacuation pllf!\Q Start Time: I ':i. 2 9 TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOVE FIGURES BY
P1, <"~ 1:s1< 3.8 LITERS/GALLON. Method of Sample Collection Time:
Chain-of-Cusfody form Started ~no)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 5th Volume.
Volume Purged (gallons) ,., 1 . ., '. " tl.S' S. L
Time (military) 143"-... -'"'" Ill, l /J:o-z.. I , I·, .
pH (S.U.) /1. Q 5-O s. I C: -S. I
Sp. Cond. (umhos/cm) 1-J.1,,. l-1, \,c." c; IL() r1 (-,, "-.7 \(\
Wafer Temp. (•c) I~ I q I ~ I' I q
Odor {subjective)• 1-1 '-l ~ u 1-1
Turbidity (subjecfive)" I f I I I
• (l)None (2)Slighf (3)Moderole ( 4)Slrong
" (l)Cleor (2)Slighlly Turbid (3)Moderolely Turbid {4)Very forbid (5)Exlremely Turbid
Commenls/Observalions/Recommendalions: ---------------------------
1,, d J\ , AJ,,t-4i>l•c4ll,
000031
FORM COMPLETED BY: .,!i.J.ltcc...--l,l~!,t'.l,~f.lJ.:l;__
DATE: -L.<.UC.kll.L.J....:.'-----
0& r form48 {3/94)
fl.
I
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Explanation of Symbols and Abbreviations
The following defines common symbols and abbreviations used in reporting technical data:
RDL Report Detection Limit MDL Method Detection Limit
TOP Top of Pipe MSL Mean Sea Level
TNTC Too Numerous Ta Count MPN Most Probable Number
BTU British Thermal Units NTU Nephelometric Turbidity Units
C Degrees Centigrade F Degrees Fahrenheit
umhos/cm micromhos/cm meq milliequivalents
kg kilogram(s) g gram(s)
mg milligram(s) ug microgram(s)
I liter(s) ml milliliters(s)
ul microliter(s) m3 cubic meter(s)
lb pound(s) ft3 cubic foot(feet)
ft foot(feet) TIC Tentatively Identified Compounds
mg/I, mg/kg Units of concentration in milligrams per liter for liquids and milligrams per kilogram for solids.
Also referred to as Parts Per Million or "ppmn when the assumption is made that the specific
gravity or density is one (1 g/ml).
ug/I, ug/kg Units of concentration in micrograms per liter for liquids and micrograms per kilograms for
solids. Also referred to as Parts Per Billion or "ppb" when the assumption is made that the
specific gravity or density is one ( 1 g/ml).
wt% Units of concentration expressed on a weight/weight basis (e.g. grams per 100 grams).
< Less Than -The number following the sign is the limit of quantitation, the smallest amount of
analyte that can be reliably determined using this test.
> Greater Than
Data Qualifiers:
A
B
C
E
J
p
X
•
TIC is a possible aldol-condensation product resulting from sample extraction, (Organics)
Analyte also detected in the method blank.
Amendable Cyanide is a negative value due to an unknown interference.
Estimated concentration due to interference.
Estimated value below RDL or estimated value for TIC. (Organics)
Concentration difference between primary and confirmation columns > 25%. (Organics) The lower
result is reported.
Matrix interference which requires dilution or prevents the reporting of a result. Detection limits have
been adjusted where applicable.
Defined in report comments .
Solid samples (i.e. soil, sludge, and solid waste) are reported on a dry weight basis unless otherwise noted.
Test results relate only to the sample tested. Clients should be aware that a critical step in a chemical or
biological analysis is the collection of the sample. Unless the sample analyzed is truly representative of the
bulk of the material involved, the test results will be meaningless. If you have any questions regarding the
proper techniques of collecting samples, please contact us. However, we cannot be held responsible for
sample integrity unless sampling has been performed by a member of our staff.
WARRANTY AND LIMITATION OF LIABILITY -The accuracy of all analytical results is warranted for the
sample as it is received by the laboratory. Warranty for the integrity of the sample begins at the time it is
placed in the possession of authorized Davis & Floyd, Inc. Laboratories personnel. All other warranties,
expressed or implied, are disclaimed. Liability is limited to the cost of the analysis.
Davis & Floyd, Inc.
AD07_0/ (07/99)
0no03i1
Davis & f-loyd, Inc. I PO Drawer 4211 I Greenwood, SC 2%48 I 81(> E. 0urs1 Avenue I Greenwood, SC 29649 I (8(i4) 229-4413 I f-ax (B64) 229-7119
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I Attachment 3
I Selected Water-Quality Plots
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I Kubal-Furr & Associates
-------------------Inner Tier Combined Influent TOC Data
3500 - -
3000
! 25001
0 '; 2000 -
~ -C .,
u 5 1500 -
(J
1 000 - - - - - - -- - - - -- - - - - - - - - -- - - - - - - -
500 -----------------
ITCI TOC Data
0+-------+-------+-------+-----!------+-------'----------'---J
1/1/93 1/1/94 1/1/95 1 /1 /96 12/31 /96
Date
12/31/97 12/31 /98 12/31/99
-------------------
Location
ITCI
Date
11 /29/94
3/7/95
5/18/95
8/22/95
11 /29/95
1/16/96
4/ 1 5/96
7/12/96
10/31/96
1/17/97
4/29/97
7/22/97
1 0/28/97
1 /22/98
5/7/98
7/21/98
1 0/20/98
1/14/99
4/8/99
8/ 1 9/99
11 /9/99
Value
2330
1800
1000
209
52
11 00
1 070
550
840
603
1560
1430
1 1 1 0
99
1310
596
550
665
1 51 0
310
1 040
Unit
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
J
JL
z
ITCI Ethylene Glycol Data
ITCI Ethylene Glycol Data
2500 ~-----------------~
~ "' E
2000
~ 1500
C: 0 :;::: .. ~ ~ 1000 u C: 0 0
500
0 -j-,-----,----+----------;------+-----
11/29/94 11/29/95 11/28/96 11/28/97 11/28/98 11/28/99
Date
-------------------Monitor Well V-23 TOC Data
V-23 TOC Data
14000 -,----------------------------------------~
12000 ----______________ OU.-2.End ______________________________________ _
1 0000 -
:::. -"' .S 8000 - - - - - - - - - - - - - - - - - - - - --
C:
0 :;:: ca ~ -; 6000 - - - - - - - - - - -- - - - - - -
" C: 0 (.)
4000 - - - - - - - - - - - -· · ·
2000 -
---------------r · ----
OU-1 Start -
0+-----------+-------------'',--------+-------+-------i'--------'
1/1/85 1/1/87 12/31/88 12/31/90 1 2/30/92
Date
1 2/30/94 1 2/29/96 12/29/98
-------------------Monitor Well V-23 2-Butanone Data (MEK)
Location Date Value Unit
V-23 8/3/89 1 . 1 mg/L
V-23 2-Butanone (MEK) 11 /9/89 0.45 mg/L
1 /5/90 0.37 mg/L
2/23/90 0.038 mg/L 4 -
8/8/90 0.56 mg/L
11/7/90 0.01 mg/L u 3.5 -- - - - - - - - - - --- -- ----- - - --
2/5/91 0.66 mg/L
5/3/91 0.46 mg/L 3 -- - - - - - - - - - - -::J'
8/9/91 0.04 mg/L u -~ ~ C) bl ~ w
11/4/91 0.05 mg/L u .5,2.5 ---£ ----- - - -N - - -- - - --- - --- --- --; ::, N 0
2/4/92 0.2 mg/L C 0 ::,
0 0 :;: 2 -l 1::.::::: 1.::::::::: 5/5/92 0.2 mg/L u "' ~
8/7/92 0.8 mg/L -C ~ 1.5 ---- -- -- - - ---11 /6/92 0.1 mg/L u C
2/3/93 0.05 mg/L u 0 0 -- - - - - - - - -- - - - --- - --5/5/93 0.25 mg/L u
8/6/93 0.044 mg/L 0.5 -11/3/93 0.01 mg/L u
2/2/94 0.25 mg/L u 0 -.
8/5/94 0.52 mg/L 6/1 /89 6/1/91 5/31 /93 5/31 /95 5/30/97 5/30/99 3/8/95 0.01 mg/L <
8/24/95 0.767 mg/L Date >
1/16/96 3.6 mg/L
7/12/96 0.5 mg/L
1/17/97 0.591 mg/L
7/22/97 0.01 mg/L <
1 /22/98 0.164 mg/L
7/21/98 0.466 mg/L
1/14/99 0.34 mg/L
7/21/99 0.27 mg/L J
-------------------Monitor Well V-23 Acetone Data
Location Date Value Unit
V-23 8/3/89 0.1 mg/L u
11 /9/89 0.295 mg/L
1 /5/90 0.3 mg/L
2/23/90 0.34 mg/L V-23 Acetone Data 8/8/90 0.31 mg/L
11 /7/90 0.01 mg/L u
2/5/91 0.52 mg/L 1 .4 ·
5/3/91 ~ ~ 0.53 mg/L " C
"' "'
8/9/91 0.48 mg/L 1 .2 - --N ~ . - --- - - - - -
~ :', 0 0 11/4/91 0.53 mg/L " .J "'
2/4/92 0.08 mg/L B C) 1 -rr .••• .s 5/5/92 0.2 mg/L u l5 0.8 8/7/92 1 . 1 mg/L E
11 /6/92 0.14 mg/L ~ E o.6 - - - - ---- -----
2/3/93 0.05 mg/L u Cl) u 5/5/93 mg/L B E 0.4 ·
8/6/93 0.025 mg/L 0
11 /3/93 0.01 mg/L u 0.2 - - - --- -
2/2/94 0.36 mg/L
8/5/94 0.52 mg/L 0
3 I 8 /9 5 0.01 mg/I 6/1 /89 6/1/91 5/31 /93 5/31/95 5/30/97 5/30/99
8/24/95 0.648 mg/I J Date 1/16/96 0.487 mg/L
7/11/96 1. 15 mg/I
1/17/97 0.818 mg/I
7/22/97 0.05 mg/I <
1 /22/98 0.01 mg/I <
7/21/98 1.22 mg/I J
1/14/99 0.005 mg/L <
7/21/99 0.27 mg/L J
- --· - - - - - - - - - - - - - - - -
Monitor Well V-23 Benzene Data
Location Date Value Unit
V-23 8/3/89 0.05 mg/L u
11 /9/89 0.005 mg/L u
1 /5/90 0.019 mg/L J
2/23/90 0.031 mg/L V-23 Benzene Data
8/8/90 0.02 mg/L u
11/7/90 0.013 mg/L 0.3 ·
2/5/91 0.022 mg/L J
5/3/91 0.013 mg/L J
8/9/91 0.04 mg/L u 0.25 . - - - - - - - - - - - --- ---- -
11/4/91 0.015 mg/L J :J'
2 / 4 /9 2 0.012 mg/L J -C) 0,2 - - - -t: - - --- - -
.. ~ .s ~ <
5/5/92 0.071 mg/L J t w • N in N :I 8/7 /92 0.05 mg/L u C: :, 0 0 :, 0
11/6/92 0.017 mg/L J 'i 0. 15 ·o Tl - - -- - - --
~
-!
2/3/93 0.006 mg/L J -C: .,
5/5/93 0.25 mg/L u u 0. 1 C: ----- ------------------ ---
8/6/93 0.004 mg/L J 0 0
11 /3/93 0.022 mg/L
2/2/94 mg/L u 0.05 --------------------0.25
8/5/94 0.022 mg/L J
3/8/95 0.011 mg/I < 0
8/24/95 0.0293 mg/I 6/1/89 6/1/91 5/31 /93 5/31 /95 5/30/97 5/30/99
1/16/96 0.0193 mg/L Sample Date
7/11/96 0.0291 mg/I
1/17/97 0.0178 mg/I
7/22/97 0.02 mg/I
1 /22/98 0.01 04 mg/I
7/21/98 0.0207 mg/L
1 /14/99 0.014 mg/L
7/21 /99 0.018 mg/L
- --· - - - - - - - - - - - - - - - -Monitor Well K-28 TOC Data
K-28 TOC Data
9000 ·r---------------------------------------,
8000 -- - - - - - - - - - -
7000 - - - - - - - - - - - - - - - -
~ 6000 -
..J -en E
; 5000 -
0 :;::
"' ~ c 4000 .. .,
u C 0
CJ 3000 -
2000 - -
1000 - -
Begin OU-2 - - - -
Remediation
l
End OU-2
' · Remediation · · · · · · · · · -
.t. . . . . . .....
Inner Tier
Start-Up
l
0f--4----+-----+-----+-----+----+----+--~=--+--+"'~l+'-~--_J
9/1 /81 9/1/83 8/31/85 8/31/87 8/30/89 8/30/91 8/29/93 8/29/95 8/28/97 8/28/99
Date
- -_, - - - - - - - - - - - - - - - -
Sheet1 Chart 1
K-28 Benzene Data
0,035 -~----------------------------------------~
:J' C)
0.03
0.025 -1-
,5, 0.02 -
C: 0 ~ ~ -C: :'l 0.015 -
C: 0 u
0.01
0,005
0+--------<----------+---------+--------~-------~-~
6/1 /89 6/ 1 /91 5/31/93 5/31/95 5/30/97 5/30/99
Date
Page 1
- --I -- - - - - -- ---- -- - -
HH-48 TCE Data
Location Date Value Unit
HH-48 8/3/89 0.16 mg/L
11/7/89 0.14 mg/L
2/5/90 0.005 mg/L u
5/ 1 /90 0.17 mg/L
8/2/90 0.15 mg/L HH-48 TCE Data 11/2/90 0.15 mg/L
2/1/91 0.15 mg/L
5/2/91 0.12 mg/L 0.25
8/2/91 0.01 mg/L u
11/1/91 0.16 mg/L
2/3/92 0.16 mg/L 0.2 - ------ - - - - ---
4/30/92 0.15 mg/L
8/3/92 0.18 mg/L ::J' 11 /3/92 0.22 mg/L E -"' 2/1 /93 0.15 mg/L .S 0.15
5/3/93 0.18 mg/L C 0
8/2/93 0.2 mg/L :;::; .. ~ 11/1/93 0.22 mg/L E -C
1/31/94 mg/L a, 0.1 · ... - - - ---- --- - - - -. . . -- --- - - --0.2 u
C
8/1 /94 0.16 mg/L 0 u
8/1 /94 0.01 mg/L
3/8/95 0.17 mg/L 0.05 · -- - - ---- -. - - - -. ------- - - -- - - - --- ------
8/23/95 0.222 mg/L
1/17/96 0.165 mg/L
7/12/96 0.179 mg/L
1/17/97 0.15 mg/L 0
7/22/97 0.09 mg/L 6/30/89 6/30/91 6/29/93 6/29/95 6/28/97 6/28/99
1 /22/98 0.1 01 mg/L Date
7/21/98 0.08 mg/L
1/14/99 0.088 mg/L
7/21/99 0.084 mg/L
- -_,_ - - -_,_ - - - - - - - - - -
HH-77 Chart 1
HH-77 TCE Data
0.45 -,--------------------------------------------,
0.4
0.35
0.3 · - - - - - - - - - - - --- - -
:;
CJ
E -0.25
C: 0
-.;
~ -~ 0,2
0
C:
0
0
0. 15
0.1
0.05
0 +. --------+----------+---------+---------+---------+--___,
6/1 /89 6/ 1 /91 5/31 /93 5/31 /95 5/30/97 5/30/99
Date
Page 1