NCD003446721_19990801_Celeanse Corporation - Shelby Fiber_FRBCERCLA RA_OU-1 Semiannual Report January - June 1999-OCR

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RECEIVED
AUG 16 1999
Operable Unit 1-Semlannual Report SUPERFUND SECTION January 1999 -June 1999
HNA Holdings, Inc.
Shelby, North Carolina
(F.K.A. Hoechst Celanese Corporation)
Document Control No. 026S8-0084
Submitted to
U.S. Environmental Protection Agency
Region IV
Atlanta, Georgia
Prepared for
HNA Holdings, Inc.
Shelby, North Carolina
August 1999
Kubal-Furr & Associates
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Contents
Iw.
Introduction ............................................................ 1
Work Performed ......................................................... 3
1st Quarter 1999 ...................................................... 3
2nd Quarter 1999 ..................................................... 4
System Performance ...................................................... 5
Inner and Outer Tier Extraction Rates ...................................... 5
Ground-Water Movement ............................................... 6
Treatment Efficiencies .................................................. 7
Maintenance Activities ................................................. 8
Analytical Test Results ..................................................... 9
Data-Quality Assessment ............................................... 9
Discussion of Analytical Test Results ...................................... 9
Review of Selected Historical Water-Quality Data ........................... 11
Closing Comments ...................................................... 14
Tables
Table 1. 1999 Sampling Matrix-HNA Holdings, Inc.-Shelby, NC
Table 2. Inner Tier Production Data (January 1999-June 1999)
Table 3. InnerTierTOC Data (January 1999 -June 1999)
Table 4. Summary of Selected CERCLA-related Water-Quality Data (1st Quarter 1999)
Table 5. Summary of Selected CERCLA-related Water-Quality Data (2nd Quarter 1999)
Table 6. Summary of Selected PEW-related Water-Quality Data (1st Quarter 1999)
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Figures
Figure L Site Plan Showing Monitoring Locatim;is and Geologic Cross Sections
Figure 2. Potentiometric Surface Map-Shallow Saprolite-January 13, 1999
Figure 3. Potentiometric Surface Map-Deep Saprolite/Upper Bedrock-January 13, 1999
Figure 4. Hydrogeologic Cross Section A-A', January 13, 1999
Figure 5. Potentiometric Surface Map-Shallow Saprolite-April 7, 1999
Figure 6. Potentiometric Surface Map-Deep Saprolite/Upper Bedrock-April 7, 1999
Figure 7. Hydrogeologic Cross Section A-A', April 7, 1999
Attachments
Attachment 1. Operation and Maintenance Data (January 1999 -June 1999)
Attachment 2. Analytical Data for the January and April 1999 Sampling Events
Attachment 3. Selected Water-Quality Plots
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HNA Holdings, lnc.-Shelby, NC-Semiannual Reporr!Page 1
Introduction
HNA Holdings, Inc. (fonnerly known as Hoechst Celanese Corporation) is currently operating
a long tenn remedial action (LTRA) system at its Shelby, North Carolina facility. This system,
designated as Operable Unit 1 (OU-1) in the Record of Decision (ROD), consists of two ground-
water extraction and treatment systems identified as the Inner Tier and Outer Tier systems. OU-1
became operational in August 1989.
The OU-1 Inner Tier system was designed to extract contaminated ground water from around a I fonner source area which was remediated as a separate operable unit (OU-2) with its own ROD.
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The Outer Tier system was designed to provide hydraulic control over ground water near the
property boundary to prevent the off-site migration of any constituents from the fonner OU-2
source area. The location of the Inner and Outer Tier systems, the fonner OU-2 source area, and the
ground-water monitoring points are shown on Figure 1.
Kubal-Furr & Associates (KF&A) has prepared this semiannual OU-1 operating summary
report for submittal to the EPA on behalf of HNA. It covers the period from January 1, 1999
through June 30, 1999 and includes infonnation on system perfonnance and the results of
analytical testing of samples collected on January 14, 1999 and April 8, 1998. It should be pointed
out that during the 1st Quarter, the laboratory inadvertantly failed to analyze the Inner Tier influent
and effluent samples for ethylene glycol. As a result, the lab collected additional Inner Tier samples
on March 2, 1999 which were analyzed for the presence of ethylene glycol in accordance with the
sampling and analysis plan.
Routine ground-water extraction and treatment continued during the semiannual reporting
period. The most significant, non-routine event was the repair and rehabilitation of monitor well H-
79. The outer casing of this well was significantly damaged by a piece of heavy equipment, and on
February 4, 1999, Kubal-Furr & Associates supervised its repair and re-development, which was
perfonned by Geologic Exploration, Inc., of Statesville, N.C. After hand-excavating the inner and
outer casings, it was determined that the PVC well casing was crimped and bent but not broken,
minimizing the concern of contamination from surface soils or surface water run-off. The well was
purged of five well volumes (approximately 35 gallons) and the purge water was noted to be very
clear, relatively sediment-free, and had no noticable odors. Upon completion of the re-development,
a piece of new Schedule 40 PVC riser pipe was coupled (no glue) onto the existing well. A new
protective steel casing was installed over the well and concreted in place. Also, two protective steel
bumper posts which had also been damaged were re-installed to provide additonal protection for the
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HNA Holdings, Inc.-Shelbv. NC-Semiannual Report/Page 2
well. Upon completion of the repairs, the purge water was disposed of at the designated
decontamination area ( decon pad).
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HNA Holdings, Inc.-Shelbv, NC-Semiannual Report/Page 3
Work Performed
As part of the OU-1 remedy, samples are collected at selected monitor wells and at points in the
ground-water treatment system. In addition, samples were collected from the PEW extraction well
system and PEW-related monitor wells. A list of sampling locations and the parameters analyzed
during the I st and 2nd Quarters are summarized in Table I. A description of the work performed
during this reporting period is provided below.
1st Quarter 1999
On January 13, 1999, water levels were measured by Kubal-Furr in a total of 'f7 monitor wells,
extraction wells, and piezometers. A total of 17 water-quality samples and 2 duplicate samples were
collected on January 14, 1999 from selected monitor wells and extraction wells. Additionally, 4
process point samples were collected. All samples were collected and analyzed by Davis & Aoyd
of Greenwood, South Carolina. As noted in the introduction, the laboratory inadvertantly failed to
analyze the Inner Tier influent and effluent samples for ethylene glycol. As a result, the lab collected
additional Inner Tier samples on March 2, 1999 which were analyzed for the presence of ethylene
glycol in accordance with the sampling and analysis plan.
OU-I Monitor Well Samvling
Thirteen monitor wells (plus 2 duplicates) were analyzed in the field for pH, temperature and
conductance; and, by the laboratory for volatile organics (VOCs) using EPA Method 8260B.
Samples from monitor wells K-28 and V-23 were also analyzed by the laboratory for TOC using
EPA Method 9060.
OU-I Process Point Sampling
Samples of Inner Tier (IT) influent and effluent were coHected for analysis of volatile organics
by Method 8260B. The Inner Tier influent and effluent samples were also analyzed by the
laboratory for total organic carbon (TOC) by Method 9060, and for ethylene glycol by GC/FID.
Samples of SBR and FP (filter press) sludge were also collected and analyzed for the full TCLP
suite of constituents.
During the reporting period, influent and effluent samples from the Inner Tier were also
collected by HNA personnel for analysis of TOC by Davis & Aoyd. These samples are collected
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HNA Holdings, /nc.-Shelby, NC-Semiannual Report/Page 4
weekly to evaluate treatment efficiency, and the results are contained in the O&M reports provided
in Attachment l. These results are also summarized in Table 3.
PEW Extraction and Monitor Well Sampling
One PEW-related monitor well (F-55) and 3 PEW extraction well samples were collected
during the 3rd Quarter. These samples were analyzed for VOCs by EPA Method 82608, for
SVOCs (semivolatile organics) by EPA Method 8270C (including biphenyl and diphenyl ether).
2nd Quarter 1999
On April 8, I 999, water levels were measured by Kubal-Furr in a total of 98 monitor wells,
extraction wells, and piezometers. Water-quality samples were collected from 2 monitor wells, and 2
process points (plus one process point duplicate) and analyzed for the parameters summarized in
Table l. The samples were collected on April 8, I 999 by Davis & Royd, who also performed the
analyses.
Monitor Well Sampling
Monitor wells K-28 and V-23 were sampled during the 2nd Quarter sampling event. These
wells were analyzed in the field for pH, temperature and conductivity; and, by the laboratory for
TOC by Method 9060.
Process Point Sampling
Samples of Inner Tier influent and effluent were collected for analysis of TOC by Method
9060 and volatile organics by EPA Method 82608. The Inner Tier influent and effluent samples
were also analyzed for ethylene glycol by GCIFID.
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HNA Holdings, /nc.-Shelby, NC-Semiannual Report/Page 5
System Performance
Detailed records of system maintenance are kept by HNA and are summarized monthly. The
monthly records for the current reporting period 'are contained in Attachment I. Summaries of
physical operating data for the Inner Tier extraction well system is presented in Table 2.
Inner Tier Extraction Rates
During the reporting period, the Inner Tier wells extracted a total of 313,991 gallons. Inner Tier
flows ranged from a low of 40,937 gallons in January, to a high of 60,188 gallons in March.
Pumping from the Inner Tier wells is limited by the capacity of the SBR treatment system, which is
designed to process about 2500 gallons of water per day. With 181 days in the reporting period, at
design capacity, pumping from the Inner Tier would have been some 452,500 gallons. Based on the
pumpage during the reporting period, the Inner Tier extraction system was producing at a rate of
about 69% of the design capacity, which represents a decrease from the previous semiannual
reporting period during which the Inner Tier produced about 73% of the design capacity rate.
Ground-Water Movement
In order to accurately predict the direction of ground-water movement, · water-level
measurements were collected from all accessible monitor wel_ls, extraction wells and piezometers on
January 13, 1999 by KF&A, and again on April 7, 1999. These data were used to construct the
potentiometric surface maps and hydrogeologic cross sections (Figures 2 thru 7).
The shallow saprolite maps (Figures 2 and 5) show the water-level contours and direction of
ground-water movement in the uppermost water-bearing zone beneath the site. The direction of
movement in this zone is to the east from upgradient areas along NC 198, towards discharge areas
along the intermittent, unnamed tributaries of Buffalo Creek. Drawdown and a capture zone are
apparent on these figures situated around the Inner Tier extraction system.
An attempt was made to separate the uppermost water-bearing zone from the deeper saprolite
and upper bedrock zone. While these maps (Figures 3 and 6) present a reasonable picture of
ground-water movement in this zone, it should be pointed out that it is giving a somewhat more
generalized picture of ground-water movement because of the well construction techniques used in
many of the wells and piezometers. The typical construction of these wells was to have relatively
long screens (20-40 ft) and extremely long sand packs in the annular space above the screens (up to
60-ft). As a result, the lower saprolite/upper bedrock maps have a number of composite head values
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HNA Holdings, lnc.-Shelby, NC-Semiannual Report/Page 6
measured along a longer screened area. However, the maps may be useful for determining the
general direction of ground-water movement
To confirm inferences made about the direction of movement and hydraulic control exerted by
the Inner Tier system, hydrogeologic cross sections were constructed from the January and
December data sets (Figures 4 and 7). The location of the cross section is shown on the site base
map, Figure 1. The east-west cross section (A-A') is constructed through the plant from upgradient
areas west of the plant to downgradient, off-site areas east of the plant. The east-west hydrogeologic
cross section shows a general direction of movement in the saprolite and upper bedrock from
upgradient areas west of the plant toward downgradient areas to the east. No appreciable downward
hydraulic gradients are apparent on this map, and the movement in the saprolite and shallow
bedrock is predominantly horizontal across the site.
Treatment Efficiencies
Two aspects of the extraction system performance were reviewed for this semiannual report: the
production rates achieved during the reporting period, and the removal efficiencies for TOC from
the Inner Tier system.
Table 3 summarizes the treatment system effectiveness for the Inner Tier in removing TOC
during the reporting period. These summaries were prepared from the water-quality data collected
weekly by the HNA on-site laboratory as presented in the monthly operating summaries
(Attachment I). During the reporting period, the Inner Tier average removal efficiency for TOC was
greater than 99%, with an average influent concentration of 1614 ppm (parts per million), and an
average effluent concentration of 6.6 ppm.
Maintenance Activities
Low flow from the Inner Tier wells is a chronic problem requiring frequent maintenance. The
actions taken to rectify the low flow problems consisted of replacing bladders, timers, air lines and
such, adjusting the controls and flow rates, and cleaning the strainers. Specific actions taken at
individual wells during the reporting period are contained in the monthly operating summaries
(Attachment 1). In addition, lower water levels in the shallow saprolite early in the year affected
Inner Tier performance, specifically IT-9, which pumped little to no water during the entire month
of January and part of February.
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HNA Holdings, Inc.-Shelby, NC-Semiannual Report/Page 7
Analytical Test Results
The analytical test results for the 1st and 2nd Quarter sampling events were evaluated using
method specific quality control criteria and, for additional guidance when necessary, the EPA's
National Functional Guidelines for organic and inorganic data review. Analytical test results, field
sampling logs, and chain-of-custody forms for the 1st and 2nd Quarter data sets are contained in
Attachment 2. A summary of selected analytical data for the 1st and 2nd Quarters is presented in
Tables 4, 5 and 6.
Data-Quality Assessment
Regarding sample collection, the sampling logs and field information provided was complete.
Several inconsistencies were noted between units in the hard copy and electronic deliverables. These
discrepancies were discussed with the laboratory, were changed in the database and hard copy, and
require no qualification of the analytical test results.
Surrogate recoveries for the 2nd Quarter for toluene were slightly below the lower control limit
(82.8% vs LCL of 84% ). In general, test results for the 1st and 2nd Quarters met all method
acceptance criteria and are considered useable for quantitative purposes.
Discussion of Analytlcal Test Results
CERCLA-Monitor Wells
Of the 13 monitor well samples analyzed during the reporting period, only four had any volatile
organics reported above the detection level (Tables 4 and 5). Of these four, only one (V-23) had
more than one individual volatile constituent reported as present above the detection level.
Monitor well V-23, located downgradient of the former OU-2 source area and just up gradient
of the Inner Tier extraction system, reportedly contained benzene (0.014 mg/L), and 2-butanone
(0.34 mg/L). Monitor wells HH-48 and HH-77, off-site and adjacent to the Elliott residence,
reportedly contained trichlorothene (TCE) at concentrations of 0.088 mg/L and 0.13 mg/L,
respectively. The presence of TCE at this location is thought to be the result of a localized source,
unrelated to activities at HNA or the former OU-2 source area.
Monitor wells K-28 and V-23 were also analyzed for TOC during the 1st and 2nd Quarters.
The V-23 test results for the 1st and 2nd Quarters were 5810 mg/Land 7760 mg/L, respectively.
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HNA Holdings, lnc.-Shelby, NC-Semiannual Report/Page 8
The TOC test results for K-28 were noted to increase from 5.9 mg/L to 43 mg/L between the 1st
and 2nd Quarters.
Process Point Samples
Inner Tier influent and effluent samples were analyzed during the ]st and 2nd Quarters for
ethylene glycol, TOC, and volatile organics. All volatiles and ethylene glycol test results for the
Inner Tier effluent sample were below the detection level of 7.0 mg/L. The 1st Quarter Inner Tier
influent sample reportedly contained the volatiles benzene (0.035 mg/L), chlorobenzene (0.033
mg/L), and 2-butanone (0.074 mg/L). The 2nd Quarter Inner Tier influent sample reportedly
contained the volatiles acetone (0.84 mg/L), benzene (0.027 mg/L), and 2-butanone (0.041 mg/L).
Inner Tier influent ethylene glycol results for the 1st and 2nd Quarters were reported at 665 mg/L
and 1510 mg/L, respectively.
The Filter Press (FP) and SBR sludges were tested for all TCLP constituents during the 1st
Quarter. The metals barium and selenium were the only TCLP constituents reported above the
detection limits, and both were detected in the FP sludge sample at 4.5 mg/L and 0.084 mg/L,
respectively. Based on these results, the sludges would not be considered characteristically
hazardous, nor would they exceed any applicable State standard for disposal in a North Carolina
landfill.
TOC test results for the Inner Tier influent samples were noted to increase between the 1st and
2nd Quarters from 1620 mg/L to 2530 mg/L, respectively. Inner Tier effluent TOC was reported at
4.1 mg/Land 8.8 mg/L for the ]st and 2nd Quarters, respectively.
PEW-Related Samples
Of the four PEW-related samples collected during the 1st Quarter, only F-55 and PEW-4 had
more than one volatile or sernivolatile constituent reported as present. Acetone (0.064 mg/L), and
benzene (0.061 mg/L) were reported as present in well F-55. Cis-1,2-dichloroethene (0.011 mg/L)
and trichloroethene (0.091 mg/L) were reported as present in PEW-4.
Two of the four wells sampled had reportable quantities of Dowtherm constituents (i.e., 1,1-
biphenyl or biphenyl ether). 1,1-biphenyl was reported as present in wells F-55 ( 10.8 mg/L), and
PEW-4 (0.012 mg/L). Biphenyl ether was reported as present in well F-55 (23.1 mg/L) and PEW-
4 (0.039 mg/L). Well F-55 also reportedly contained the semivolatile constituents dibenzofuran
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HNA Holdings, Inc.-Shelby, NC-Semiannual Report/Page 9
(0.078 mg/L), naphthalene (034 mg/L), phenol (0.049 mg/L), 4-methylphenol (0.18 mg/L), and 2-
methylnaphthalene (0.71 mg/L).
Review of Selected Hlstorlcal Water-Quality Data
Attachment 3 contains plots of selected water-quality constituents for various monitor wells and
process points. The choice of locations and constituents was based on a review of the water-quality
database, in particular those locations having any meaningful data to plot. In general, only those
monitoring locations within a few hundred feet of the former OU-2 source area have any significant
number of water-quality constituents reported above the detection limits. In an attempt to assess
long-term improvement in water-quality conditions resulting from source removal and ground-water
recovery, the following locations and constituents were selected:
• Inner Tier Combined Influent TOC and ethylene glycol test results. The Inner Tier TOC ·
increased between the 1st and 2nd Quarter, reversing a trend established in early 1997.
Similarly, the Inner Tier ethylene glycol data increased during the 1st and 2nd Quarters
although no long-term trends have been established.
• Monitor Well V-23 TOC, 2-butanone (MEK), acetone and benzene. The V-23 TOC data
began trending downward from a high 6f8000 mg/Lin mid-1989 to less than 1000 mg/Lin
early 1992. Since that time, the TOC data have shown several wide swings in concentration.
TOC concentrations at V-23 decreased during the 1st Quarter and rose again during the 2nd
Quarter.
The V-23 MEK data have generally fluctuated in a narrow range below 1 mg/L,"with 12 of
29 data points below the detection level. The values for MEK decreased during the 1st
Quarter sampling event but no discemable trend is apparent in the data set.
The V-23 acetone test results have generally fluctuated in a narrow range below 0.6 mg/L
since 1989. Acetone concentrations at V-23 have been below the detection level in three of
the past four quarters. The previous quarter's test result (3rd Quarter 1998) was reportedly
the highest concentration detected at this well although the value was flagged as estimated
due to a matrix interference.
• While more than half the benzene data for V-23 is flagged as estimated or below the
detection limit, the past eight sampling events have been quantitative and show benzene to be
fluctuating in a narrow range of from 10 to 30 µf!IL.
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HNA Holdings, lnc.-Shelby, NC-Semiannual Report/Page JO
• Monitor well CC-33 benzene data. The water-quality plots for monitor well CC-33, just
south of the Inner Tier capture zone, have shown a continual improvement in water-quality
conditions as indicated by the benzene concentrations. This improvement began in late
1991, just after start up of the Inner Tier extraction system. Benzene peaked at about the
mid-point in the OU-2 remediation (late 1991), and has continued to decline since that time.
The most recent test result was below the detection limit.
• Monitor well K-28 TOC and benzene data. TOC and benzene have both shown a stairstep
decrease in concentration beginning about the time the OU-2 source remediation began in
January of 1991. While benzene has shown a general decline during this period, a slight
upward trend has been noted since the 1st Quarter of 1997.
• Monitor well HH-48 and HH-77 TCE data. The HH-48 TCE test results have declined
from a concentration of 0.222 mg/L in August of 1995, to 0.088 mg/L during the most
recent quarter (1st Quarter 1999). HH-77 had been fluctuating in the range of 0.05 to 0.15
mg/L until the July 1996 sampling event when it peaked at 0383 mg/L. TCE at HH-77 was
noted to decrease from 0.225 mg/L to 0.13 mg/L between the 3rd Quarter of 1998 and the
1st Quarter of 1999, and a long-term downward trend is apparent at this location.
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HNA Holdings, lnc.-Shelby, NC-Semiannual Report/Page I I
Closing Comments
The extraction well production data and the analytical test results for the monitor wells and
process points were generally found to be consisterit with historical information, and no unusual or
unsuspected contamination was identified during the reporting period. Treatment efficiencies at the
Inner Tier for removal of TOC remained consistently greater than 99%, and no volatiles were
detected in either the 1st or 2nd Quarter Inner Tier effluent samples.
The next CERCLA-sampling events are scheduled for the 3rd and 4th Quarters of 1999, with
another PEW-related sampling scheduled for the 3rd Quarter. The next scheduled semiannual
report is to be submitted to the agency by March 1, 2000.
Kubal-Furr & Associates
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Table 1. 1999 Sampling Matrix-HNA Holdings, lne.-Shelby
1st 9!:!arter 2nd ~arter 3rd 9!:!arter 4th Q!;!arter
Monitoring Toe voe Eth. Glycol Toe voe Eth. Glycol TOe voe Eth. Glycol TOC voe Eth. Glycol
Location (9060) (82608) (GC/FIO) (9060) (8260B} {GC/FID) (9060) (82608) (GC/FID} (9060} (82608) (GC/FID)
Process Points
rra ..j ..j ..j ..j ..j ..j ..j ..j ..j ..j ..j ..j
ITEF ..j ..j ..j ..j ..j ..j ..j ..j ..j ..j ..j ..j
OTO ,I. (OT Pume!ng Discontinued on 4/21/98)
OTEF ..j
SBR Sludge (Full TQP}11
FP Sludge (Full TQ..P)11
,.,onitor Wells
C-49 ..j ..j
K-26 ..j ..j ..j ..j ..j ..j
P-58
T-35 ..j ..j
V-23 ..j ..j ..j ..j ..j ..j
M-54
CC-33 ..j ..j
EE-58 ..j ..j
FF-34
FF-62 ..j ..j
GG-61 ..j ..j
HH-48
HH-77 ..j ..j
voe svoe voe svoc
(82608) (8270C) (82608) (8270C)
PEW-Related Same!_es
PEW-1 ..j ..j ..j ..j
1'£W-3 ..j ..j ..j ..j
P£W-4
8-34
F-55 ..j ..j ..j ..j
G-SO
G-88
K-59
K-79
Notes: 1 / TCLP Analyses as specified in Attactn'mnt 2: of most~ approved Sarrping & Analysis Plan (KF&A, April 1998)
HNA Holdings, lnc.-Shelby, NC
OU-/ Semiannua.l Report(Jan. '99 • June'99)
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January 1999 February 1999
Total Total
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Table 2. Inner Tier Production Data
Jan. '99 --June '99
HNA Holdings, lnc.-Shelby, NC
March 1999 Aprll 1999
Total Total
____!'i!!!_ Gallons ADF• Gallons ~ Gallons ~ Gallons AOF'
IT-1 2,647 85 3,077 110 4,036
IT-2 770 25 849 30 1,036
IT-3 2 421 78 1 219 44 1 091
IT-4 3,556 115 5,077 181 2,972
IT-5 10,809 349 7,989 285 10,835
IT_,, 3 458 112 3 729 133 4 588
IT-7 3,538 114 4,536 162 6,368
IT-8R 13,736 443 12,690 453 13,721
IT-9 2 0 11 082 396 15 541
40,937 50,248 60,188
• AOF: Average Dally Flow based on HNA production records (Attachment 1 ),
Calculated as totaf flow divided by the number of days In the month.
130 4,199 140
33 835 28
35 2 742 91
96 2,954 98
350 9,545 318
148 3 487 116
205 6,300 210
443 12,330 411
501 15 218 507
57,610
-- -
' May 1999
Total
Gallons 2.Qf_
3,828 123
809 26
3 195 103
2,729 88
8,885 287
3 275 106
3,735 120
15,383 496
17 601 568
59,440
- -- -
June 1999 Jan.-June '99
Total
Gallons ADF' Total Gallons
3,153 105 20,940
823 27 5,122
2 174 72 12 842 •
2,323 77 19,611
8,303 277 56,366
1 740 58 20 277
3,203 107 27,680
12,715 424 80,575
11 134 371 70 578
45,568 313,991
HNA Holdings, /nc.-Shelby, NC
OU-1 Semiannual Report(Jan. '99-June '99)
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Table 3. Inner Tier TOC Data
Jan. '99 -June '99
HNA Holdings, lnc.-Shelby~ North Carolina
(all results reported in ppm)
Influent Effluent % Reduction
Date
116199 1430 2 99.9
1113199 3090 3 99.9
1120199 2050 5 99.8
1127199 1930 3 99.8
212199 1930 4 99.8
2110199 1380 5 99.6
2117199 1530 4 99.7
2125199 1920 5 99.7
311199 1670 4 99.8
3110199 1600 6 99.6
3117199 1510 7 99.5
3124199 1490 6 99.6
3131199 1560 7 99.6
411199 1580 NIA
4114199 NIA 6
4121199 1680 8 99.5
4128199 1570 9 99.4
515199 1210 8 99.3
5112199 1350 NIA
5119199 1310 10 99.2
5126199 1450 9 99.4
612199 1580 9 99.4
618199 1450 10 99.3
6116199 1450 11 99.2
6124199 1330 9 99.3
6130199 1010 8 99.2
Average: 1614 6.6 99.6
(Note: 411199, 4114199 and 5112/99 data not used to calculate averages)
HNA Holdings, Inc.-Shelby, NC
OU-I Semiannual Report (Jan. '99 -June '99)
-------------------
Table 4. Summary of Selected Water-Quality Constituents (1st Quarter 1999)
(All results reported in milligrams per liter)
K-28 V-23
Total Organic Carbon 5.9 5810
Ethylene glycol NA11 NA
Vo/a tile Organics
Benzene 0.010 0.014
2-butanone (MEK) <0.010 0.34
Chlorobenzene <0.005 <0.005
Trichloroethene <0.005 <0.005
Notes: 1 / NA = Sample not analyzed for indicated constituents
HH-48 HH-77
NA NA
NA NA
<0.005 <0.005
<0.010 <0.010
<0.005 <0.005
0.088 0.13
Inner Tier
Influent
1620
665
0.035
0.074
0.033
<0.005
Inner Tier
Effluent
4.1
<7.0
<0.005
<0.010
<0.005
<0.005
HNA Holdi11gs, hlc.-Shelby, NC
OU-1 Semia11nual Report (Ja11 '99-Ju11e '99)
-------------------
Table 5. Summary of Selected Water-Quality Constituents (2nd Quarter 1999)
(All results reported in milligrams per liter)
K-28 V-23
Total Organic Carbon (mg/L) 43 7760
Ethylene glycol (mg/L) NA 11 NA
Volatile Organics (mg/Ll
Acetone NA NA
Benzene NA NA
2-butanone (MEK) NA NA
Notes: 1 / NA = Sample not analyzed for indicated constituent(s)
Inner Tier
Influent
2530
1510
0.84
0.027
0.041
Inner Tier
Inner Tier Effluent
Effluent Dupe
12.7 8.8
<7.0 <7.0
<0.010 <0.010
<0.005 <0.005
<0.005 <0.005
HNA Holdings, Jnc.-Shelby, NC
OU-I Semiannual RepoTI (Jan. '99 -June '99)
-------------------
Table 6. Summary of Selected PEW-Related Water Quality Constituents (1st Quarter 1999)
(All results reported in milligrams per liter)
F-55 PEW-1
Semivolatile Organics
1 , 1 biphenyl 10.8 <0.010
Biphenyl ether 23.1 <0.010
dibenzofuran 0.078 <0.010
naphthalene 0.34 <0.010
phenol 0.049 <0.010
4-methylphenol (p-cresol) 0.18 <0.010
2-methylnaphthalene 0.71 <0.010
Vo/a tile Organics
Acetone 0.064 <0.010
Benzene 0.061 <0.005
cis-1,2-dichloroethene <0.005 <0.005
Trichloroethene <0.005 0.0074
PEW-3
<0.010
<0.010
<0.010
<0.010
<0.010
<0.010
<0.010
<0.010
<0.005
<0.005
<0.005
PEW-4
PEW-4 (Dupe)
0.012 <0.010
0.039 0.034
<0.010 <0,010
<0.010 <0.010
<0.010 <0.010
<0.010 <0.010
<0.010 <0.010
<0.010 <0.010
<0.005 <0.005
0.011 0.011
0.091 0.093
HNA Holdings. lnc.-Shelby, NC
OU-1 Semiannual Report (Ja11. '99 -Ju11e '99)
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Figure 1-Site Location
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Shdby, North Carolina
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IT-1 = <780.67
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IT-5 = 779.13
IT -6 = 779.54
IT-7 = 788.82
IT-SR = Nol Measured
IT-9 = Not Measured
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Figure 2-Potentiometrio 5urfaoe Map
Shallow 5aprolite-January 13, 1999
HNA Holding5, Inc.
Shelby, t-!orth Carolina
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January 1:3, 1999
HNA Holdinge, Inc.
Sho!:lby, North Carolina
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A. A A .. A .. A ... A A• A .... A A ......... A A .. A A. A A A A A,_ .... A •• A A .......... A• A ... A A A A ... A ...... A ... A. A A ..... A A A A .. ,_ A A A A A A A A• A A A ... A• ... A• A ... A ... t A ...... A ......... • AIA. A A,._,._ 1 A A ...... h • ,. ........................................................................................................................................................... ,. .............................................................................................................................. ~
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............................................................................................................ ·.· .................................................................................. •,. .......................................................... • .. •,,. ................ · ......... · .................. •,.• ............. · ... · ..................................................................................... ·.· ....................................................................................................... · ........................ •,. ................... ·~· ... ...
A ... A A ... A A ... A A • A A .. A • • A A .. .. A A A A ... A • A A • ,_ A ... A ... • • A A A A A A • .. ... • ... .. ... A A ... A A A A A • .. A A A .. ... A A A ... ... A ... A ... • A ... • ... ... A • A A ... A • A ... .. A • .. A A A A • • .. • .. A ... A .. A A .. .. A • A "' A A .. ...
A A A A ... ... A A A A A ... ... A • • A A A ... A A A .. A A A .. ... A ... A A A A .. A ... • A • A A ... A .. A • A A ... A ... • ... • • • • ... • A .. .. ... A A .. A A ... A ... A A • • A A ... .. A ... A A A A .. A A A • A A • • A A A .. ... ~ A A A .. A A A A ... .. • ... • ... , • ......................................... • ... •." ................. ""..,"'..,· ............................................... • ....................................... ,. ......... • ... • ............. • ... • ................................................................ • ... • ................................................................................................................................................................................................................................................................................... • ... • .................. •. H. H. :77· •
... ... ... A • .. A • A ... A • A A A A • .. • A • ... A A • A .. ... ... A ... • A ... .. • A ... .. ... • A A • ... ... ... A A • A .. • A A • A ... ... ... A A .. • A A ... • .. A ... • A • A A A ... ... A ... A • • A A A A ... • A A • ... • • A A ... A • .. .. .. A • A .. A A A • • A
Legend
0
• ...... ,. • .................................................................... • ... • ...................................................................... • ... • ...................... • .................. ,. ............................. • ........ •,,. ................................... • ............ ·715 68
Horizontal Scale in Feet .. '"' ... "' "' ...... • ·."' ... '"' ... •. ·.'"' • ... "". • .......... '"' ............. "' ......... • ... "'."' ... ·."' ......... " ... "' ... '"' ........ • ... '"' ....... "". • ........ ·."' ... • • "'• .......... "' •"' ... "' ... • • .... · • .. :.. ......
400 800
Line of equal fluid potential (ft msl) 1:23 Bedrock (dashed where inferred)
. . . . . ... . .. . . . ... . . .
. . . ... . . . . .. . . . . . .
. . . ...
850.00
830.00
810.00
790.00
770.00
750.00
730.00
710.00
690.00
670.00
Potentiometric Surface D
Inferred direction of ground-water i
Saprolite
Screened Interval of Well Kubal-Furr & Associates
-Environmental Consultants -
Figure 4-Hydrogeologic Cross-Section
A-A'-January 13, 1999
movement HNA Holdings, Inc.
Sh~fby, North Carolin.a
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CP Cl' t t>1 ~ 0
e,
fj
Legend
Monl!arWeH 0 • Water-level (ft msr) .0. ... Pi&zometor ♦ ◊ Out« TIBI' Extraction WeU " + Inner rier Extraction wen -¢-+ PEWEictraction Well
■ C Rnidential Supply WeU -' ' /foo/ Vll'aler-ltwel Contour , -
(dashedwher. W.rr~ * □ Bulldlng/Struct\Jre
0 N OJ
Morvtor Well Cluster
Abnd. Plezometet
Abnet Outer Tier Extraction W.I
Abn'd. Inner Tter Extraction \Nell
Abnd. PEW Ex1ract.On Wei
Abnd. RHldentlal Supply Wed
Creela'Stream
Not used ln Contouring
8 0
0
Scale in Feet
400
_,
-fl
000
' ' '
I,, ,
I_,. -~ I
0 <S) t--
'
'
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\1 Cro~
' If}
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\ 'I
O GG-25 754.31 ,
Kubal-Furr & Associates
-Environmental Consultants -
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0 -!, --.,
~ <Ii a-,;i_"'
loner Tier Extraction Well Water-Levels
IT-1 = 782.02
IT-2 = <776.45
IT-3 = <781.46
IT-4 = <775.18
IT-5 = 777.69
IT-6 = <778.64
IT-7 = 788.48
IT-BR = 795.62
IT-9 = Not Measured
'
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Figure 5-Potentlometrio 5urfaoe Map
Shallow 5aprolite-April 7, 1999 .
HNA Holdinge, Inc.
Sh~/by, North Carolina
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$,
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--
MnnitocWell • Water-lewel (ft ms!)
A Pie.zometer
◊ Outer nor Extraction Well
+ Inner r1e1 Extraction Well + PEW Extraction WeD
C Residential Supply 'Mtb
Water-level Contour /fool (dllll\ed wi.re hten'•d)
['jJ Build~tructure
\
\
0
A
♦
* -Q-
■ , .. , ,
*
Moritor Well Cluster
Abnc!. Piezometer
Abnci. Outer Tier Extraction Wei
Abnd. Inner Tier Extraction Well
Abnd. PEW Extraction Vllel
Abnd. Residential Suppty Well
Creek/Stream
Not used In Contouring
0
Scalo in Feet
400
~ C)
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, ----·o.
\
\
\
\
\
\ \ '/ .A. PZ-10 \ \
74',.77 \ \
\ \
\
\
\
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\
\ _/,---;
7901~:il lll~[iJ1tit~m i")\
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L-::::-::~':--,=::::;:::=s~-~~·~ 0 1~-1=· -:-: cc,,:,:.,.,./Uil;0· 15101 (' \\ . ... <, ':,:;'i OGG-!.
I \
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800
e~~ =" ,ll ~ ;;:::: C' • ~1 [754.02
Groundwater
freatment-
Ft11cilit,y A· PZ-9
[:;;'I:·:~:-:[ ',, \ L 759.01
::.:~·-:·.-==: ;!!li \ 34 7
•... ·1 .. E .• ~ .. 1 .. ·1•.·.:! .. 6 ..•..•. 1 ?~ I ·.62 ~ }::/\[ ' PZ-1
'?:; >_:._·_::_:::_::;::·:,~ I ' \ 7P60Z-.002 ~.,, -_.2-~· ;ji t.t-4\ 0-'·----, OT !'
775.66 -___ ..-
1
768 tine
'7"'==~!"762.41
OT-1A ,. ,.
766 74·
· , .-=Runyan I
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DD-58 e
761.76 ~19
■ Crot't!,,
\I
' C)
te
Kubal-Furr & Associates
-Environmental Consultants -
/ 1--'
I f --
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Figure 6-Potentiometrio 5urfaoe Map
Deep 5aprolite/Upper 6edrook-
April 7, 1999
HNA Holdings, Inc.
Sh~lby, North Carolina
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850.00
830.00
810.00
790.00
770.00
750.00
730.00
710.00
690.00
,,I -810
--
A
Plant Area --1----------------------j~'::..-::_-::._--------------Wastewater Treatment Area
,,
~
D-27
827.92
D-35
827.54
D-56
827.55
Line of equal fluid potential (ft ms!)
(dashed where inferred)
Potentiometric Surface
Inferred direction of ground-water
movement
G-50
812.48
Bedrock
Saprolite
Screened Interval of Well
J-28
806.40
a,
C :::;
>, -c: Q) a. e a.
Kubal-Furr & Associates
-Environmental Consultants -
A' 850.00
830.00
810.00
790.00
770.00
750.00
730.00
710.00
690.00
670.00
Figure 7-Hydrogeologic Cross-Section
A-A'-April 7, 1999
HNA Ho/dingo, Inc.
Shelby, North Carolina
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I Attachment 1
I Operation and Maintenance Data
January-June, 1999
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I Kubal-Furr & Associates
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I January 1999 O&M Data
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I Kubal-Furr & Associates
I
I INNER TIER
DAILY FLOW
I JAN. ' U9i lic1 LI:2. I.Y. LH 1H. 1H. 1H. 1H. II:i
I 01/01/99 88 23 60 82 325 106 104 643 0
01/02/99 113 24 128 210 337 108 104 675 0
01/03/99 83 22 169 115 296 90 99 425 0
01/04/99 67 23 154 57 328 119 106 1 0
I 01/05/99 0 24 98 54 313 106 107 480 0
01/08/99 70 24 84 54 333 108 109 530· 0
01/07/99 91 24 82 58 332 110 111 582 2
01/08/99 93 24 118 68 338 113 106 475 0
01/09/99 83 23 103 66 323 105 111 246 0
I 01/10/99 96 24 70 69 292 107 112 40 0
01/11/99 37 24 83 79 388 112 115 541 0
01/12/99 87 24 76 87 341 109 113 657 0
01/13/99 31 25 74 93 344 113 115 648 0
I 01/14/99 81 26 78 104 353 115 119 667 0
01/15/99 112 25 94 112 357 114 121 658 0
01/16/99 108 25 71 106 360 110 116 639 0
01/17/99 103 24 93 112 345 106 113 613 0
01/18/99 98 25 97 112 347 108 113 616 0
I 01/19/99 107 25 0 111 365 113 117 665 0
01/20/99 99 26 18 123 375 112 116 642 0
01/21/99 99 25 55 211 378 113 118 500 0
01/22/99 33 25 58 124 367 113 118 263 0
I 01/23/99 82 25 93 272 370 114 118 336 0
01/24/99 81 26 94 209 356 114 118 282 0
01/25/99 87 25 80 66 352 113 118 17 0
01/26/99 100 27 65 66 363 117 120 518 0
01127/99 103 26 54 73 382 118 120 576 0
I 01/28/99 96 26 49 84 368 118 118 516 0
01/29/99 105 27 43 124 359 119 119 185 0
01/30/99 109 27 42 204 364 119 122 0 0
01/31/99 105 27 38 251 358 116 122 0 0
I AVG: 85 25 78 115 349 112 114 443 0
I TOTAL: 2647 770 2421 3556 10809 3458 3538 13736 2
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INNER TIER COMBINED INFLUENT #2 ITCI
PAGE NO.1 I JAN.1999
DATE: FLOW: PH: COD: TSS: TOC:
GPD pH ppm ppm ppm
01/01/99 1431 5.4 6740 4 I
01/02/99 1699 5.3 6900 6
01/03/99 1299 5.2 3330 10
01/04/99 855 5.3 4880 16 I 01/05/99 1182 5.2 6250 10
01/06/99 1412 5.5 4420 6 1430
01/07/99 1392 5.5 5410 13
01/08/99 1335 5.3 6160 20 I 01/09/99 1060 5.2 7300 11
01/10/99 810 5.2 10550 9
01/11/99 1379 5.2 9890 14 I 01/12/99 1494 5.4 13350 5
01/13/99 1443 5.4 7140 1 3090
01/14/99 1543 5.4 5130 14
01/15/99 1593 5.4 6300 10 I 01/16/99 1535 5.4 6270 8
01/17/99 1509 5.4 6140 4
01/18/99 1516 5.4 6300 11 I 01/19/99 1483 5.3 6580 14
01/20/99 1511 5.4 5500 10 2050
01/21/99 1499 5.4 6640 15
01/22/99 1101 5.4 6820 27 I 01/23/99 1410 5.3 5480 36
01/24/99 1280 5.4 4590 9
01/25/99 858 5.3 5860 25
01/26/99 1376 5.2 8100 5 I 01/27/99 1452 5.4 5080 7 1930
01/28/99 1376 5.4 5490 10
01/29/99 1081 5.4 5870 4 I 01/30/99 987 5.2 9500 14
01/31/99 1017 5.1 9260 2.1
AVG: 1320 5.3 6685 12 2125 I MAX: 1699 5.5 13350 36 3090
MIN: 810 5.1 3330 1 1430
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I GROUNDWATER MONTHLY MONITORING:
INNER TIER EQUALIZATION TANK: ITEQT
I PAGE NO. 2
JAN.1999
DATE: PH: COD: OT WATER ADDED '
pH ppm gal
I 01/01/99 7.4 6900 188
01/02/99 7.4 6330
01/03/99 7.5 5600
I 01/04/99 7.4 4170 563
01/05/99 7.5 4730
01/06/99 7.5 4160
I 01/07/99 7.5 3720
01/08/99 7.0 3860
01/09/99 7.5 5500 675
01/10/99 7.4 5400
I 01/11 /99 7.5 5240
01/12/99 7.5 4600
01/13/99 7.2 5850
01/14/99 7.5 4580
I 01/15/99 7.2 5240
01/16/99 7.3 5460
01/17/99 7.4 5920
I 01/18/99 7.3 6400
01/19/99 7.2 4960
01/20/99 6.5 4680
01/21/99 7.4 5340 563
I 01/22/99 7.6 4950
01/23/99 7.5 4690
01/24/99 7.6 4480
01/25/99 7.9 5640 75
I 01/26/99 7.5 6590
01/27/99 7.6 4980 263
01/28/99 7.5 5000
I 01/29/99 7.2 6760
01/30/99 7.5 4870
01/31/99 7.3 5930
I AVG: 7.4 5243 388
MAX: 7.9 6900 675
MIN: 6.5 3720 75
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GROUNDWATER MONTHLY MONITORING: I
AFTER PLATE SEPARATOR BEFORE SBR: SBRI
PAGE NO. 3 I JAN.1999
DATE: PH: COD: TSS:
pH ppm ppm
01/01/99 5.4 7660 20 I
01/02/99
01/03/99 5.4 3890 20
01/04/99 5.6 5200 8 I 01/05/99
01/06/99 5.5 4070 16
01/07/99 I 01/08/99 5.5 3770 24
01/09/99 5.8 5350 12
01/10/99
01/11/99 5.4 3830 8 I 01/12/99
01/13/99 5.3 5680 4
01/14/99
01/15/99 6.0 5260 20 I 01/16/99
01/17/99 5.7 5170 12
01/18/99 I 01/19/99
01/20/99 5.9 4510 28
01/21/99 5.5 5690 16
01/22/99 I 01/23/99 5.4 4380 4
01/24/99
01/25/99 5.4 5960 24
01/26/99 I 01/27/99 5.5 5040 20
01/28/99
01/29/99 5.4 4410 4 I 01/30/99
01/31/99 5.4 5040 24
AVG: 5.5 4995 16 I MAX: 6.0 7660 28
MIN: 5.3 3770 4
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I GROUNDWATER MONTHLY MONITORING:
SBR MIXED LIQUOR: SBRML
I PAGE NO. 4
JAN.1999 SETT. SLUDGE 5/DAY
DATE: PH: NH3N: PO4: DO: MLSS: MLVSS: SOLIDS: WASTED . F/M: F/M:
pH ppm ppm ppm ppm ppm ml/I gal ratio ratio
I 01/01/99 8.2 164 28.0 3.6 1560 140 54 0.44
01/02/99 8.2 149 24.4 3.9 1600 140 0 0.00
01/03/99 8.1 171 20.0 4.6 1748 150 0 0.20
I 01/04/99 8.1 176 24.0 5.0 1164 150 202 0.40
01/05/99 8.2 116 17.0 5.5 1876 140 202 0.00 0.21
01/06/99 8.2 144 22.4 4.6 1832 1536 130 202 0.20 0.16
I 01/07/99 8.2 125 13.8 4.3 1900 130 202 0.00 0.16
01/08/99 8.1 141 25.4 4.3 1780 150 202 0.19 0.16
01/09/99 8.1 141 18.8 3.4 1968 150 202 0.24 0.13
01/10/99 8.1 139 15.2 3.5 1888 150 0 0.00 0.13
I 01/11/99 8.2 190 24.0 4.7 1812 150 102 0.19 0.12
01/12/99 8.1 133 17.0 4.3 2108 150 102 0.00 0.12
01/13/99 8.1 139 23.6 4.8 1888 1588 130 202 0.27 0.14
01/14/99 8.1 154 11.2 3.7 2228 130 202 000 0.09
I 01/15/99 8.1 150 44.0 4.0 1912 160 94 0.24 0.14
01/16/99 8.1 175 20.0 4.0 1912 160 0 0.00 0.10
01/17/99 8.2 112 18.0 3.9 1868 150 200 0.25 0.15
I 01/18/99 8.1 100 16.8 4.7 2168 170 0 0.00 0.10
01/19/99 8.3 121 21.7 5.5 1976 170 0 0.00 0.10
01/20/99 8.3 135 17.6 4.3 1908 1568 160 102 0.21 0.09
01/21/99 8.2 116 14.0 4.1 2192 150 102 0.23 0.14
I 01/22/99 8.2 111 16.0 4.6 2160 150 142 0.00 0.09
01/23/99 8.3 126 24.4 4.7 2168 150 142 0.18 0.12
01/24/99 8.2 122 20.8 4.3 2172 150 142 0.00 0.12
01/25/99 8.4 144 30.5 4.6 2152 150 142 0.25 0.13
I 01/26/99 8.2 139 20.4 4.8 1708 150 142 0.00 0.09
01/27/99 8.3 130 24.2 4.2 2172 1756 150 142 0.21 0.13
01/28/99 8.0 122 14.8 4.1 1980 150 142 0.00 0.09
I 01/29/99 8.3 154 26.2 4.9 1968 150 142 0.20 0.13
01/30/99 8.2 130 18.8 4.8 1988 150 175 0.00 0.08
01/31/99 8.3 137 23.2 4.3 1904 180 162
I AVG: 8.2 139 21 4 1925 1612 150 124 · 0.13 0.12
MAX: 8.4 190 44 6 2228 1756 180 202 0.44 0.21
MIN: 8.0 100 11 3 1164 1536 130 0 0.00 0.08
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GROUNDWATER MONTHLY MONITORING: I
SBR EFFLUENT:(DECANT) #4 SBRE
PAGE NO. 5 I JAN.1999 WAS. NH3N PHOS.
DATE: FLOW: COD: TSS: TSS ADDED: ADDED:
GPO ppm ppm ppm gal lbs
01/01/99 2039 120 40 10100 1 1 I
01/02/99 0
01/03/99 2064 115 32 0 1
01/04/99 2550 134 48 12570 0 0 I 01/05/99 0 10080 2 2
01/06/99 1950 178 100 . 8630 0 0
01/07/99 0 11330 2 2-I 01/08/99 2301 163 75 9640 0 0
01/09/99 2370 160 80 10280 1 1
01/10/99 0 1 2
01/11/99 2124 125 40 9510 0 0 I 01/12/99 0 13350 1 2
01/13/99 1875 154 10 8560 1 2
01/14/99 0 9260 0 2
01 /15/99 2209 174 60 10910 0 0 I 01/16/99 0 0 0
01/17/99 2339 142 528 11850 0 1
01/18/99 0 2 1 I 01/19/99 0 0 0
01/20/99 2625 185 10 8250 0 2
01/21/99 2775 176 60 10360 1 2
01/22/99 0 9850 1 2 I 01/23/99 1997 150 30 9230 1 . 2
01/24/99 0 1 2
01/25/99 2052 169 90 9560 0 0
01/26/99 0 0 0 I 01/27/99 1875 145 70 8320 0 0
01/28/99 0 8630 2 2
01/29/99 1913 130 20 8120 0 0 I 01/30/99 0 10650 1 1
01/31/99 2241 155 100 7340 1 1
AVG: 1203 151 82 9843 1 1 I MAX: 2775 185 528 13350 2 2
MIN: 0 115 10 7340 0 0
• DID NOT PROCESS SBR. I
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I GROUNDWATER MONTHLY MONITORING
INNER TIER CARBON FILTER EFFLUENT #8ITEF
I PAGE NO. 7
JAN.1999
DATE: PH: COD: TOC: TSS: '
pH ppm ppm ppm
I 01/01/99
01/02/99
01/03/99
I 01/04/99
01/05/99
01/06/99 8.5 67 2 20
I 01/07/99
01/08/99
01/09/99
01/10/99
I 01/11/99
01/12/99
01/13/99 8.4 80 3
01/14/99
I 01/15/99
01/16/99
01/17/99
I 01/18/99
01/19/99
01/20/99 8.1 149 5
01/21/99
I 01/22/99
01/23/99
01/24/99
01/25/99 I 01/26/99
01/27/99 8.2 103 3
01/28/99
I 01/29/99
01/30/99
01/31/99
I AVG: 8.3 100 3 20
MAX: 8.5 149 5 20
MIN: 8.1 67 2 20
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DAILY REFERENCE SHEET: I
DATE: IT. EQ. PLT. DEC. DEC. WAS MIX MIX MIX NIT PHOS MIX FIM I JAN. INF. TNK. SEP. LIQ LIQ LIQ ADD ADD LIQ WAS 5/DAY
llil @12. @12. @12. @12. lls. --1Sli MLll , NII eHQll. GALS. LSS. 5EL GALS. E1M AYJ3..
1 6740 6900 7660 120 40 10100 1560 164 28.0 1 1 140 54 0.44
2 6900 6330 1600 149 24.4 1 1 140 0 0.00 I 3 3330 5600 3890 115 32 1748 171 20.0 0 1 150 0 0.20
4 4880 4170 5200 134 48 12570 1165 176 24.0 0 0 150 202 0.40
5 6750 4730 10080 1876 116 17.0 2 2 140 202 0.00 0.21
I 6 4420 4160 4070 179 100 8630 1832 144 22.4 0 0 130 202 0.20 0.16
7 5410 3720 11330 1900 125 13.8 2 2 130 202 0.00 0.16 I 8 6160 3860 3770 163 75 9640 1780 141 25.4 0 0 150 202 0.19 0.16
9 7300 5500 5350 160 80 10280 1968 141 18.8 1 1 150 202 0.24 0.13
10 10550 5400 1888 139 15.2 1 2 150 0 0.00 0.13
11 9890 5240 3830 125 40 9510 1812 190 24.0 0 0 150 102 0.19 0.12
12 4940 4600 13350 2108 133 17.0 1 2 150 102 0.00 0.12 I 13 7140 5850 5880 154 10 8560 1888 139 23.6 1 2 130 202 0.27 0.14
14 5130 4580 9260 2228 154 11.2 0 2 130 202 0.00 0.09
15 6300 5240 5260 174 60 10910 1912 150 44.0 0 0 160 94 0.24 0.14
16 6270 5460 1912 160 20.0 0 0 160 0 0.00 0.10
17 6140 5970 5170 142 528 11650 1868 112 18.0 0 1 150 200 0.25 0.15 I 18 6300 6400 2168 100 16.8 2 1 170 0 0.00 0.10
19 8560 4960 1976 121 21.7 0 0 170 0 0.00 0.10
20 5500 4680 4510 180 10 8250 1908 135 17.6 0 2 160 102 0.21 0.09
21 6640 5340 5690 176 60 10360 2192 116 14.0 1 2 150 102 0.23 0.14
22 6620 4950 9850 2160 111 16.0 1 2 150 142 0.00 0.09
23 5480 4690 4380 150 30 9230 2168 126 24.4 1 2 150 142 0.18 0.12 I 24 4590 4480 9170 2172 122 20.8 1 2 150 142 0.00 0.12
25 5860 5840 5960 169 90 9560 2152 144 30.5 0 0 150 142 0.25 0.13
28 8100 6590 1708 139 20.4 0 0 150 142 0.00 0.09
27 5080 4980 5040 145 70 8320 2172 130 24.2 0 0 150 142 0.21 0.13
28 5490 5000 8630 1980 122 14.8 2 2 150 142 0.00 0.09 I 29 5870 6760 4410 130 20 8120 1968 154 28.2 0 0 150 142 0.20 0.13
30 9500 4870 10650 1968 130 18.8 1 1 150 175 0.00 0.08
31 9260 5930 5040 155 100 7340 1904 137 23.2 1 1 180 162 0.24 0.13
AVG: 6430 5245 4717 143 77 9060 1925 138.4 21.2 1 1 150 124 0.13 I MAX: 10550 6900 7660 180 528 13350 2228 190.0 44.0 2 2 180 202 0.44
MIN: 3330 3720 0 0 0 0 1165 100.0 11.2 0 0 130 0 0.00
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GROUNDWATER MONTHLY MONITORING:
RAINFALL DATA
JAN 199 .
DATE J.1'11.,;.t1ES1 uAx
01/01/99 0.00
01/02/99 2.00
01/03/99 o.oo
01/04/99 0.00
01/05/99 0.00
01/06/99 0.00
01/07/99 0.00
01/08/99 0.10
01/09/99 o.oo
01/10/99 0.00
01/11/99 0.00
01/12/99 o.oo
01/13/99 o.oo
01/14/99 0.40
01/15/99 o.oo
01/16/99 o.oo
01/17/99 0.30
01/18/99 0.10
01/19/99 0.00
01/20/99 0.00
01/21/99 0.00
01/22/99 o.oo
01/23/99 2.00
01/24/99 0.00
01/25/99 0.00
01/26/99 0.00
01/27/99 0.00
01/28/99 0.00
01/29/99 0.10
01/30/99 0.00
01/31/99 0.40
TOTAL 5.40
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
A\, IIUI•
DATE WELL# PROBLEM DATE ACTION
1/5/99 #8 LOW FLOW 1/5/99 NEW EXHUSTER
1/6/99 #1 LOW FLOW 1/6/99 NEW METER
1/20/99 #3 LOW FLOW 1/20/99 NEW METER
MECHANIC
PHIL
PHIL
PHIL
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- - - - - - - - - -·--· ·--

-

-

-

-

-
Well
OT-ZR
OT-3
OT-4
OT-5
OT-6
OT-6A
OT-7
OT-8
Thermometer
Operational? **
X
X
X
X
X
X
X
X
Monthly O&M Plan Checklist
HNA Holdings, Inc., Shelby, NC
Heat Lamp
Operational? **
X
X
X
X
X
X
X
X
Other Operational Items/Comments
(,.. Temperature and Heat Lamp checks October thru April only)
Form Completed by: __________ T:_:0:,.:N_,_Y;_::_BRc;.Y:.:.Ac.:NT.:.:... ________ _
Date: __________ .:..:11_4:,:_l.::.9,c.9 _________ _
Quarterly O&M Plan Checklist-HNA Holdings, lnc./Shelby, NC Form Completed by: TONY BRYANT
Date: 1 /1 /99
Open Sample Energize Verify De-energize Close SarTlpe Verify Heater Secure Well
Port Pump Discharge Pump Port Operation Vault Comments
Outer Tier Well
OT-ZR X X X X X X X
OT-3 X X X X X X X
OT-4 X X X X X X X
OT-5 X X X X X X X
OT-6 X X X X X X X
OT-6A X X X X X X X
OT-7 X X X X X X X
OT-8 X X X X X X X
Energize Energize Energize Energize Energize
Ground-Water AS Blower Transfer Pump Transfer Pump Transfer Pump Transfer Pump
Treatment Sys. Y-V-1008 Y-P-1007A Y..P-1007B Y..P-1008A Y-P-1008B Comments
X X X X X
--- -- - - - -- ------ - --
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I February 1999 O&M Data
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I Kubal-Furr & Associates
I
I INNER TIER
DAILY FLOW
I-FEB. ' fili II:1 lI:2. II:.3. ~ 1H 1H 1H. rr:a II:9.
I 02/01/99 118 27 43 430 368 122 131 0 0
02/02/99 110 27 35 212 369 119 127 193 0
02/03/99 109 27 3 133 392 119 122 160 0
I 02/04/99 82 27 0 138 388 118 119 454 0
02/05/99 112 30 0 143 363 120 117 572 0
02/06/99 112 27 0 152 339 118 109 512 0
02/07/99 112 30 0 163 398 138 130 592 1
02/08/99 91 31 0 158 382 136 126 611 0
I 02/09/99 109 29 0 103 329 121 109 524 0
02/10/99 97 29 18 217 251 140 136 633 0
02/11/99 108 31 57 357 54 136 137 638 3533
02/12/99 103 31 71 362 17 138 142 648 593
I 02/13/99 73 31 69 364 78 134 144 633 631
02/14/99 3 31 67 356 0 136 144 631 646
02/15/99 81 31 67 333 0 133 144 615 601
02/16/99 127 32 30 294 319 137 141 634 546
02/17/99 131 32 0 254 339 136 144 630 504
I 02/18/99 122 32 51 58 335 140 173 647 398
02/19/99 112 31 95 33 328 137 228 640 411
02/20/99 118 32 95 129 327 134 193 637 314
02/21/99 116 32 76 79 330 0 223 311 440
I 02/22/99 137 33 63 87 325 0 210 0 254
02/23/99 135 27 62 108 334 166 225 64 270
02/24/99 124 0 48 94 299 177 195 0 167
02/25/99 135 45 65 92 330 195 222 418 424
02/26/99 135 43 66 86 339 193 224 452 461
I 02/27/99 127 35 70 69 307 181 196 421 409
02/28/99 138 36 68 75 349 205 225 420 479
I AVG: 110 30 44 181 285 133 162 453 396
I TOTAL: 3077 849 1219 5077 7989 3729 4536 12690 11082
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INNER TIER COMBINED INFLUENT #2 ITCI
I PAGE NO.1
FEB.1999
DATE: FLOW: PH: COD: TSS: TOG:
GPD pH ppm ppm ppm
I 02/01/99 1239 5.2 7970 10
02/02/99 1192 5.2 5570 12 1930
02/03/99 1065 5.3 6260 10
I 02/04/99 1326 5.4 6320 16
02/05/99 1457 5.4 4160 5
02/06/99 1369 5.2 6310 7
I 02/07/99 1564 5.5 3300 17
02/08/99 1535 5.5 4180 3
02/09/99 1324 5.5 3450 10
02/10/99 1521 5.5 3856 2 1380
I 02/11/99 5051 5.5 3440 7
02/12/99 2105 5.4 4780 20
02/13/99 2157 5.4 4050 12
02/14/99 2014 5.4 3710 1
I 02/15/99 2005 5.4 2720 20
02/16/99 2260 5.3 4570 15
02/17/99 2170 5.4 4670 6 1530
02/18/99 1954 5.5 4680 7
I 02/19/99 2015 5.3 4840 15
02/20/99 1979 5.4 4370 20
02/21/99 1607 5.3 4010 10
I 02/22/99 1109 5.4 3650 13
02/23/99 1391 5.4 4910 20
02/24/99 1104 5.4 5130 13
02/25/99 1926 5.5 5340 10 1920
I 02/26/99 1999 5.6 4730 10
02/27/99 1815 5.4 3890 9
02/28/99 1995 5.5 5090 4
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I AVG: 1795 5.4 4641 11 1690
MAX: 5051 5.6 7970 20 1930
MIN: 1065 5.2 2720 1 1380
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GROUNDWATER MONTHLY MONITORING: I
INNER TIER EQUALIZATION TANK ITEQT
PAGE NO. 2 I FEB.1999
DATE: PH: COD: OT WATER ADDED '
pH ppm. gal
07/01/97 7.4 6440 I 07/02/97 7.4 4000
07/03/97 7.6 5040
07/04/97 7.5 4950 I 07/05/97 7.3 4180
07/06/97 7.5 5120
07/07/97 7.2 3760
07/08/97 7.4 3560 I 07/09/97 7.4 2700 375
07/10/97 7.4 2630
07/11/97 7.4 3820 188 I 07/12/97 7.5 2670
07/13/97 7.4 3030
07/14/97 7.4 3210 188
07/15/97 7.4 2990 188 I 07/16/97 7.4 2570 94
07/17/97 7.4 3880 150
07/18/97 7.3 3980 155
07/19/97 7.3 4680 I 07/20/97 7.4 3710
07/21/97 7.3 3540
07/22/97 7.5 2670 I · 07/23/97 7.4 2590
07/24/97 7.4 2360
07/25/97 7.5 3770 375
07/26/97 7.6 4900 441 I 07/27/97 7.6 3580
07/28/97 7.5 4670
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AVG: 7.4 3750 239
MAX: 7.6 6440 441 I MIN: 7.2 2360 94
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I GROUNDWATER MONTHLY MONITORING:
AFTER PLATE SEPARATOR BEFORE SBR: SBRI
I PAGE NO. 3
FEB.1999
DATE: PH: COD: TSS:
pH ppm ppm
I 02/01/99
02/02/99 5.8 5640 12
02/03/99
I 02/04/99
02/05/99 5.5 3920 12
02/06/99
I 02/07/99 5.7 4180 40
02/08/99 5.9 4040 4
02/09/99 6.1 3260 28
02/10/99 6.1 2630 4
I 02/11/99 5.9 2880 44
02/12/99 5.9 2620 8
02/13/99 6.3 3160 16
02/14/99 6.1 2940 12
I 02/15/99 6.6 2810 4
02/16/99 6.2 1930 4
02/17/99 6.3 2390 8
02/18/99 5.7 3370 20
I 02/19/99 5.9 4580 20
02/20/99 6.4 3310 16
02/21/99 6.1 3900 12
I 02/22/99 5.9 3280 12
02/23/99
02/24/99 5.9 2360 8
02/25/99 5.6 3240 4
I 02/26/99 5.6 4320 20
02/27/99 5.7 3360 25
02/28/99 5.6 3970 16
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AVG: 5.9 3395 15
I MAX: 6.6 5640 44
MIN: 5.5 1930 4
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GROUNDWATER MONTHLY MONITORING: I
SBR MIXED LIQUOR: SBRML
PAGE NO. 4 I FEB.1999 SETT. SLUDGE 5/DAY
DATE: PH: NH3N: PO4: DO: MLSS: MLVSS: SOLIDS: WASTED F/M: F/M:
pH ppm ppm ppm ppm ppm ml/I gal ratio ratio
02/01/99 8.3 110 18.0 3.5 2108 180 0 0.00 I 02/02/99 8.3 143 21.7 4.8 1972 1596 160 202 0.25
02/03/99 8.3 134 15.2 3.5 2032 180 0 0.00
02/04/99 8.4 167 8.0 5.2 2084 180 202 0.00 I 02/05/99 8.3 149 29.9 5.2 2308 180 202 0.15 0.08
02/06/99 8.2 122 30.0 4.1 1944 160 0 0.00 0.08
02/07/99 8.4 130 20.0 4.0 2052 200 202 0.18 0.07 I 02/08/99 8.5 113 10.8 5.0 1932 180 202 0.19 0.10
02/09/99 8.4 75 5.0 5.4 2272 180 202 0.13 0.13
02/10/99 8.4 150 16.0 4.5 2040 1656 180 202 0.11 0.12
02/11/99 8.3 123 11.0 5.1 ·2052 180 202 0.12 0.15 I 02/12/99 8.3 153 21.6 4.8 2024 180 202 0.12 0.13
02/13/99 8.4 135 12.6 5.5 2004 180 202 0.14 0.12
02/14/99 8.4 102 14.8 5.5 2040 180 202 0.13 0.12
02/15/99 8.4 151 11.6 4.5 1912 180 202 0.13 0.13 I 02/16/99 8.4 130 24.0 6.7 1976 1548 200 202 0.09 0.12
02/17/99 8.3 132 14.6 5.1 2000 200 202 0.11 0.12
02/18/99 8.3 90 14.7 5.1 2176 200 202 0.14 0.12
02/19/99 8.4 124 21.2 4.4 2104 200 0 0.19 0.13 I 02/20/99 8.3 125 18.0 5.4 2048 200 202 0.14 0.13
02/21/99 8.3 113 12.6 5.8 2140 200 202 0.16 0.15
02/22/99 8.4 104 12.4 5.1 2204 200 202 0.13 0.15 I 02/23/99 8.4 113 18.0 5.7 1772 1364 180 202 0.00 0.13
02/24/99 8.4 141 26.4 5.3 1844 180 202 0.11 0.11
02/25/99 8.3 105 17.0 5.6 1988 180 202 0.14 0.11
02/26/99 8.3 139 17.6 6.1 2276 180 202 0.17 0.11 I 02/27/99 8.2 167 16.0 5.3 1888 200 190 0.16 0.12
02/28/99 8.3 148 14.6 5.5 2052 210 200 0.17 0.15
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AVG: 8.3 128 17 5 2044 1541 186 173 0.12 0.12
MAX: 8.5 167 30 7 2308 1656 210 202 0.25 0.15 I MIN: 8.2 75 5 4 1772 1364 160 0 0.00 0.07
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I GROUNDWATER MONTHLY MONITORING:
SBR EFFLUENT:(DECANT) #4 SBRE
I PAGE NO. 5
FEB.1999 WAS. NH3N PHOS.
DATE: FLOW: COD: TSS:TSS ADDED: ADDED:
GPO ppm ppm ppm gal lbs
I 07/01/97 0 1 1
07/02/97 2014 159 20 8290 0 0
07/03/97 0 1 1
I 07/04/97 0 7250 0 2
07/05/97 2113 165 30 8080 0 0
07/06/97 0 0 0
07/07/97 2423 110 368 11370 0 0
I 07/08/97 2823 138 20 8800 2 2
07/09/97 2415 117 70 8540 2 2
07/10/97 2158 120 20 9580 0 2
I 07/11/97 2370 113 30 7930 1 2
07/12/97 2721 110 40 9020 0 0
07/13/97 2438 124 10 7650 1 2
07/14/97 2333 144 10 6870 2 2
I 07/15/97 2330 145 20 7570 2 2
07/16/97 2365 137 20 9200 0 0
07/17/97 2333 135 10 8090 0 2
07/18/97 2420 126 70 8020 2 2
I 07/19/97 2748 159 70 1 1
07/20/97 2475 122 100 8300 1 1
07/21/97 2400 116 50 8300 1 1
I 07/22/97 2250 115 50 9830 1 2
07/23/97 0 9800 1 2
07/24/97 1908 125 30 9100 0 0
07/25/97 2562 113 10 8230 2 2
I 07/26/97 2075 120 125 9520 1 2
07/27/97 2447 133 100 7810 0 1
07/28/97 1774 103 70 8180 0 0
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AVG: 1925 128 58 8555 1 1
I MAX: 2823 165 368 11370 2 2
MIN: 0 103 10 6870 0 0
• DID NOT PROCESS SBR.
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GROUNDWATER MONTHLY MONITORING I
INNER TIER CARBON FILTER EFFLUENT #8ITEF
PAGE NO. 7 I . FEB.1999
DATE: PH: COD: TOC: TSS: '
pH ppm ppm ppm
02101/99 I 02/02199 8.2 123 4 20
02103/99
02/04/99 I 02/05/99
02106/99
02107/99 I 02108/99
02109/99
02110/99 8.4 90 5
02111/99 I 02/12/99
02/13/99
02114/99
02115/99 I 02116/99
02117/99 8.4 83 4
02118/99
02119/99 I 02120/99
02121/99
02122199 I 02123/99
02124/99
02/25/99 8.2 104 5
02126/99 I 02/27/99
02128/99
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AVG: 8.3 100 5 20 I MAX: 8.4 123 5 20
MIN: 8.2 83 4 20
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I DAILY REFERENCE SHEET:
I DATE: IT. EQ. PLT. DEC. DEC. WAS MIX MIX MIX NIT PHOS MIX F/M
FEB. INF. TNK. SEP. LIQ LIQ LIQ ADD ADD LIQ WAS 5/DAY
1ffl ~ ~ ~ ~ !S.S. ..:ms. MUS. ' NII ~ GALs. L.B.S. ~ GALs. ELM AYJJ..
I 1 7970 6440 2109 110 18 1 1 180 0 0.00
2 5570 4000 5640 159 20 8290 1972 143 21.7 0 0 160 202 0.25
3 6266 5040 2032 134 15.2 1 1 180 0 0.00
4 6320 4950 7250 2064 167 8.0 0 2 180 202 0.00
5 4160 4180 3920 165 30 8080 2309 149 29.9 0 0 180 202 0.15 0.08
I 6 6310 5120 1944 122 30.0 0 0 160 0 0.00 0.08
7 3300 3760 4180 110 368 11370 2052 130 20.0 0 0 200 202 0.18 0.07
8 4180 3560 4040 136 20 8800 1932 113 10.8 2 2 180 202 0.19 0.10
9 3450 2700 3260 117 70 8540 2272 75 5.0 2 2 180 202 0.13 0.13
10 3656 2670 2630 120 20 9580 2040 150 16.0 0 2 180 202 0.11 0.12
11 3440 3820 2880 113 30 7930 2052 123 11.0 1 2 180 202 0.12 0.15
I 12 4780 2670 2620 110 40 9020 2024 153 21.6 0 0 180 202 0.12 0.13
13 4050 3030 3160 124 10 7650 2004 135 12.6 1 2 180 202 0.14 0.12
14 3710 3210 2940 144 10 6870 2040 102 14.8 2 2 180 202 0.13 0.12
15 2720 2990 2810 145 20 7570 i912 151 11.6 2 2 180 202 0.13 0.13
16 4570 2570 1930 137 20 9200 1976 130 24.0 0 0 200 202 0.09 0.12
I 17 4670 3880 2390 135 10 8090 2000 132 14.6 0 2 200 202 0.11 0.12
18 4680 3980 3370 126 70 8020 2176 90 14.7 2 2 200 202 0.14 0.12
19 4840 4680 4580 159 70 2104 124 21.2 1 1 200 0 0.19 0.13
20 4370 3710 3310 122 100 6300 2048 125 18.0 1 1 200 202 0.14 0.13
21 4010 3540 3900 116 50 6300 2140 113 12.6 1 1 200 202 0.16 0.15
I 22 3850 2670 3280 115 50 9830 2204 104 12.4 1 2 200 202 0.13 0.15
23 4910 2590 9800 1772 113 18.0 1 2 180 202 0.00 0.13
24 5130 4360 2360 125 30 9100 1844 141 26.4 0 0 180 202 0.11 0.11
25 5340 3770 3240 113 10 8230 1968 105 17.0 2 2 180 202 0.14 0.11
26 4730 4900 4320 120 125 9520 2276 139 17.6 1 2 180 202 0.17 0.11
I 27 3690 3580 3360 133 100 7810 1868 167 16.0 0 1 200 190 0.18 0.12
28 5090 4870 3970 103 70 8180 2052 148 14.6 0 0 210 200 0.17 0.15
I AVG: 4842 3823 3124 118 54 7897 2044 128.1 16.9 1 1 188 173 0.12
MAX: 7970 6440 5640 165 368 11370 2308 167.0 30.0 2 2 210 202 0.25
MIN: 2720 2570 0 0 0 0 1772 75.0 5.0 0 0 160 0 0.00
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GROUNDWATER MONTHLY MONITORING:
RAINFALL DATA
DATE l"ISIS. INCHES/UIU:
02/01/99 1.60
02/02/99 0.00
02/03/99 o.oo
02/04/99 0.00
02/05/99 0.00
02/06/99 0.00
02/07/99 0.00
02/08/99 0.00
02/09/99 0.50
02/10/99 0.00
02/11/99 0.00
02/12/99 0.00
02/13/99 o.oo
02/14/99 0.00
02/15/99 o.oo
02/16/99 o.oo
02/17/99 0.70
02/18/99 o.oo
02/19/99 1.00
02/20/99 o.oo
02/21/99 0.00
02/22/99 o.oo
02/23/99 o.oo
02/24/99 o.oo
02/25/99 o.oo
02/26/99 0.00
02/27/99 0. 00 .
02/28/99 0.00
TOTAL 3.80
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MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
~vllVI~
DATE WELL# PROBLEM DATE ACTION
213/99 #8 LOW FLOW 213/99 REPLACED BLADDER
218/99 #3 LOW FLOW 218/99 CLEANED LINES
211/99 WATER TABLE CAME UP STARTED
TO218/99 #9 NO FLOW 218/99 PUMPING
2110/99 #3 LOW FLOW 2110/99 NEW METER & CLEANED LINES
2/23/99 116 NO FLOW 2123/99 CLEANED LINES
2/23/99 #8 NO FLOW 2123/99 CLEANED LINES & NEW METER
2123/99 #9 LOW FLOW 2/23/99 CLEANED PROBE
MECHANIC
PHILP.
PHILP.
PHILP.
PHILP.
PHILP.
PHILP.
Well
OT-2R
OT-3
OT-4
OT-5
OT-6
OT-GA -
OT-7
OT-8
Thermometer
Operational? ••
X
X
X
X
X
X
X
X
Monthly O&M Plan Checklist
HNA Holdings, Inc., Shelby, NC
Heat Lamp
Operational? ••
X
X
X
X
X
X
X
X
Other Operational Items/Comments
(** Temperature and Heat Lamp checks October thru April only)
Form Completed by: _________ _:T..=Oc..N:..cY--=Bc;.R'-'Y'-A"--N'-'-T------,-----
Date: _________ __:2::./...:.1:..;/9:..:9:__ ________ _ -------------------
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I March 1999 O&M Data
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11
Kubal-Furr & Associates
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I INNER TIER
DAILY FLOW
I MARCH. ' tlli 1I=1 lI:.2. 1H II=4 1H. 1H. [H lLll. II.:i
I 03/01/99 133 35 59 78 332 184 221 355 474
03/02/99 111 35 58 84 336 189 219 59 483
03/03/99 28 19 60 103 345 190 226 0 496
03/04/99 0 0 56 136 321 151 200 39 485
I 03/05/99 122 45 61 173 343 150 210 501 510
03/06/99 137 42 61 162 353 153 209 587 498
03/07/99 136 41 57 156 348 151 187 581 458
03/08/99 137 37 53 171 350 149 192 581 484
I 03/09/99 139 34 48 130 352 149 201 564 524
03/10/99 137 34 43 125 348 150 210 545 563
03/11/99 138 34 7 87 365 150 142 530 570
03/12/99 136 34 6 84 369 147 250 520 559
03/13/99 137 35 18 97 377 150 210 525 583
I 03/14/99 131 34 33 94 363 147 204 510 583
03/15/99 130 34 32 82 297 148 198 511 585
03/16/99 145 33 30 74 364 145 187 520 587
03/17/99 149 33 32 76 346 146 187 520 601
I 03/18/99 148 33 3 74 358 146 192 518 598
03/19/99 146 33 0 82 346 144 210 515 589
03/20/99 148 33 0 65 356 144 243 515 586
03/21/99 145 34 0 69 363 146 247 489 590
I 03/22/99 140 35 0 72 365 143 219 480 593
03/23/99 141 34 41 72 364 141 219 444 596
03/24/99 141 35 43 75 366 140 223 431 533
03/25/99 138 35 42 92 367 138 236 419 537
03/26/99 138 35 42 75 368 137 238 452 569
I 03/27/99 107 27 33 55 300 118 187 373 249
03/28/99 141 39 46 69 310 112 191 350 26
03/29/99 152 35 42 80 352 140 232 446 349
03/30/99 151 34 41 69 345 143 114 434 540
I 03/31/99 154 35 44 111 366 147 164 407 143
AVG: 130 33 35 96 350 148 205 443 501
I TOTAL: 4036 1036 1091 2972 10835 4588 6368 13721 15541
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I INNER TIER COMBINED INFLUENT #2 ITCI
I PAGE NO.1
MARCH.1999
DATE: FLOW: PH: COD: TSS: TOG:
GPD pH ppm ppm ppm
I 03/01/99 1871 5.5 5320 20 1670
03/02/99 1574 5.5 4400 8
03/03/99 1467 5.5 6120 6
I 03/04/99 1388 5.5 3550 7
03/05/99 2115 5.5 4800 5
03/06/99 2202 5.5 4730 12
I 03/07/99 2115 5.5 5460 2
03/08/99 2154 5.7 4230 15
03/09/99 2141 5.2 4810 15
03/10/99 2155 5.3 5340 6 1600
I 03/11/99 2023 5.5 4000 14
03/12/99 2105 5.4 4240 17
03/13/99 2132 5.4 4800 35
03/14/99 2099 5.3 4480 41
I 03/15/99 2017 5.3 3650 10
03/16/99 2085 5.3 4110 15
03/17/99 2090 5.5 4970 11 1510
03/18/99 2070 5.5 3580 18
I 03/19/99 1977 5.3 4000 29
03/20/99 2090 5.4 4030 10
03/21/99 2083 5.4 3930 11
I 03/22/99 2027 5.2 3590 7
03/23/99 2052 5.3 4810 12
03/24/99 1987 5.4 5370 4 1490
03/25/99 2004 5.3 3720 11
I 03/26/99 2054 5.3 4200 11
03/27/99 1449 5.2 4040 14
03/28/99 1284 5.4 5020 28
03/29/99 1828 5.3 6100 30
I 03/30/99 1871 5.3 4370 10
03/31/99 1571 5.4 5190 3 1560
AVG: 1938 5.4 4547 14 1566
I MAX: 2202 5.7 6120 41 1670
MIN: 1284 5.2 3550 2 1490
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GROUNDWATER MONTHLY MONITORING: I
INNER TIER EQUALIZATION TANK: ITEQT
PAGE NO. 2 I MARCH.1999
DATE: PH: COD: OT WATER ADDED '
pH ppm gal
03/01/99 7.4 3390 189 I 03/02/99 7.5 3480 390
03/03/99 7.3 4710
03/04/99 7.3 3790 I 03/05/99 7.4 3460 563
03/06/99 7.4 3020 375
03/07/99 7.4 3240 374 I 03/08/99 7.4 3450 263
03/09/99 7.1 4150
03/10/99 7.4 4980 188
03/11/99 7.6 3890 112 I 03/12/99 7.9 3820 150
03/13/99 7.6 4450 150
03/14/99 7.6 4000
03/15/99 7.6 3070 38 I 03/16/99 7.4 2650 188
03/17/99 7.6 4190 263
03/18/99 7.5 3510 75
03/19/99 7.8 3450 I 03/20/99 8.3 3440
03/21/99 8.3 2730
03/22/99 8.4 3650 375 I · 03/23/99 8.2 4090 563
03/24/99 8.3 4580 300
03/25/99 8.4 3300 188
03/26/99 8.4 3630 113 I 03/27/99 7.3 3320
03/28/99 7.2 3910
03/29/99 7.2 3800 263
03/30/99 7.5 4570 563 I 03/31/99 7.5 4650 375
AVG: 7.7 3754 275 I MAX: 8.4 4980 563
MIN: 7.1 2650 38
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I GROUNDWATER MONTHLY MONITORING:
AFTER PLATE SEPARATOR BEFORE SBR: SBRI
I PAGE NO. 3
MARCH.1999
DATE: PH: COD: TSS:
pH ppm ppm
I 03/01/99 5.5 3650 12
03/02/99 5.5 3450 20
03/03/99
I 03/04/99 5.5 3410 16
03/05/99 6.1 3690 44
03/06/99 6.7 3670 16
03/07/99 6.2 3460 8
I 03/08/99 5.7 3710 4
03/09/99 5.9 2710 8
03/10/99 5.3 3280 4
I 03/11/99 5.6 4280 12
03/12/99 5.6 3750 8
03/13/99 7.4 4140 12
03/14/99 5.4 4040 8
I 03/15/99 5.6 3210 8
03/16/99 5.5 3990 4
03/17/99 5.9 3400 16
03/18/99 5.4 3990 8
I 03/19/99 5.5 3870 4
03/20/99 6.1 3690 28
03/21/99 5.6 3070 12
I 03/22/99 5.6 4300 24
· 03/23/99 5.9 4000 4
03/24/99 6.8 3030 4
03/25/99 5.6 3400 8
I 03/26/99 5.6 3550 4
03/27/99 5.5 3040 12
03/28/99 5.4 3650 28
03/29/99 5.5 4600 16
I 03/30/99 5.7 4850 8
03/31/99 5.6 4350 16
AVG: 5.8 3708 13
I MAX: 7.4 4850 44
MIN: 5.3 2710 4
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GROUNDWATER MONTHLY MONITORING: I
SBR MIXED LIQUOR: SBRML
PAGENO.4 I MARCH.1999 SETT. SLUDGE 5/DAY
DATE: PH: NH3N: PO4: DO: MLSS: MLVSS: SOLIDS: WASTED F/M: F/M:
pH ppm ppm ppm ppm ppm ml/I gal ratio ratio
03/01/99 8.3 116 17.0 6.0 1896 180 202 0.17 I
03/02/99 8.4 169 20.6 5.4 2448 1884 180 202 0.13
03/03/99 8.3 133 10.8 5.1 2460 180 202 0.00
03/04/99 8.4 180 20.0 6.3 1700 180 202 0.18 I 03/05/99 8.3 119 16.0 4.8 2148 180 202 0.15 0.13
03/06/99 8.3 122 28.0 6.2 1828 180 202 0.18 0.13
03/07/99 8.3 191 14.0 5.8 1728 160 202 0.18 0.14 I 03/08/99 8.4 82 16.4 5.4 1720 160 202 0.19 0.18
03/09/99 8.3 106 16.2 6.5 1692 160 202 0.14 0.17
03/10/99 8.4 146 16.4 5.7 2568 1976 150 202 0.11 0.16
03/11/99 8.3 223 12.4 6.5 2468 150 202 0.15 0.16 I 03/12/99 8.4 136 17.4 6.0 2376 150 202 0.14 0.15
03/13/99 8.3 132 24.0 5.0 1828 150 202 0.20 0.15
03/14/99 8.3 125 17.6 3.4 2048 150 202 0.18 0.16
03/15/99 8.3 108 12.8 6.5 1976 150 202 0.14 0.16 I 03/16/99 8.3 128 17.0 4.8 2108 1648 150 202 0.17 0.17
03/17/99 8.4 120 17.4 5.6 2412 150 202 0.13 0.16
03/18/99 8.4 134 20.0 4.5 1896 150 202 0.19 0.16
03/19/99 8.4 149 25.0 4.6 2412 150 202 0.14 0.15 I 03/20/99 8.4 154 22.0 4.4 1984 160 202 0.17 0.16
03/21/99 8.5 167 28.1 4.5 2044 140 200 0.13 0.15
03/22/99 8.4 113 24.7 6.2 1940 150 202 0.20 0.17 I . 03/23/99 8.5 175 27.5 5.5 2160 1696 150 202 0.16 0.16
03/24/99 8.5 105 22.0 5.5 2280 150 202 0.12 0.16
03/25/99 8.4 129 24.6 6.2 1852 150 202 0.16 0.16
03/26/99 8.5 102 20.1 7.2 1824 150 202 0.17 0.16 I 03/27/99 8.5 148 21.5 5.6 1640 150 202 0.16 0.16
03/28/99 8.6 129 24.0 6.6 1668 130 202 0.19 0.16
03/29/99 8.5 138 28.0 6.7 2520 140 202 0.16 0.17
03/30/99 8.3 175 14.0 6.2 1780 1424 150 202 0.24 0.19 I 03/31/99 8.5 116 20.1 5.9 1760 150 202 0.22 0.20
AVG: 8.4 138 20 6 2038 1726 156 202 0.16 0.16 I MAX: 8.6 223 28 7 2568 1976 180 202 . 0.24 0.20
MIN: 8.3 82 11 3 1640 1424 130 200 0.00 0.13
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I GROUNDWATER MONTHLY MONITORING:
SBR EFFLUENT:(DECANT) #4 SBRE
I PAGE NO. 5
MARCH.1999 WAS. NH3N PHOS.
DATE: FLOW: COD: TSS: TSS ADDED: ADDED:
GPO ppm ppm ppm gal lbs
I 03/01/99 2550 158 110 10140 2 2
03/02/99 2336 152 30 8320 0 0
03/03/99 0 8660 3
I 03/04/99 2187 142 20 8130 0 2
03/05/99 2765 134 60 7520 1 2
03/06/99 2250 116 40 8640 0 0
03/07/99 2288 100 40 8940 0 2
I 03/08/99 2288 125 50 9190 2 2
03/09/99 2206 162 20 8540 2 2
03/10/99 2461 146 30 10340 1 2
I 03/11/99 2082 175 60 9280 1 2
03/12/99 2153 155 10 9340 0 2
03/13/99 2393 140 70 1 0
03/14/99 2380 143 90 8700 1 1
I 03/15/99 2311 138 40 11980 1 2
03/16/99 1875 145 30 8490 1 2
03/17/99 2298 140 190 10410 1 2
03/18/99 2250 155 40 10090 1 2
I 03/19/99 1977 132 50 10820 0 0
03/20/99 1785 128 230 9100 0 1
03/21/99 1928 115 140 3770 0 0
I 03/22/99 2029 136 100 7800 1 2
03/23/99 2052 150 30 11040 0 0
03/24/99 1940 109 20 7820 1 2
03/25/99 1875 129 60 10030 0 0
I 03/26/99 1875 104 20 7700 2 2
03/27/99 2138 132 50 5200 0 0
03/28/99 1950 115 60 9070 1 2
03/29/99 1988 149 30 10060 0 0
I 03/30/99 1962 135 30 9240 0 2
03/31/99 1918 147 30 5500 1.0 2.0
AVG: 2080 137 59 8795 1 1
I MAX: 2765 175 230 11980 2 3
MIN: 0 100 10 3770 0 0
• DID NOT PROCESS SBR.
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GROUNDWATER MONTHLY MONITORING I
INNER TIER CARBON FILTER EFFLUENT #8 ITEF
PAGE NO. 7 I ,. MARCH.1999 . ,'
DATE: PH: COD: TOC: TSS: '
pH ppm ppm ppm
03/01/99 8.1 131 4 50 I
03/02/99
03/03/99
03/04/99 I 03/05/99
03/06/99
03/07/99 I 03/08/99
03/09/99
03/10/99 7.8 131 6
03/11/99 I 03/12/99
03/13/99
03/14/99
03/15/99 I 03/16/99
03/17/99 8.2 135 7
03/18/99
03/19/99 I 03/20/99
03/21/99
03/22/99 I · 03/23/99
03/24/99 8.1 94 6
03/25/99
03/26/99 I 03/27/99
03/28/99
03/29/99
03/30/99 I 03/31/99 8.4 116 7
AVG: 8.1 121 6 50
MAX: 8.4 135 7 50 I MIN: 7.8 94 4 50
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I DAILY REFERENCE SHEET:
I DATE: IT. EQ. PLT. DEC. DEC. WAS MIX MIX MIX NIT PHOS MIX F/M
MAR. INF. TNK. SEP. LIQ LIQ LIQ ADD ADD LIQ WAS 5/DAY
fill CQ12. CQ12. CQ12. CQ12. Ill. .ns. MUS ' llllI et:IQS. ~ LBS. SE!. ~ ELM AYSJ.
1 5320 3390 3650 158 110 10140 1896 116 17.0 2 2 180 202 0.17
I 2 4400 3480 3450 152 30 8320 2448 169 20.6 0 0 180 202 0.13
3 6120 4710 8660 2460 133 10.8 0 3 180 202 0.00
4 3550 3790 3410 142 20 8130 1700 180 20.0 0 2 180 202 0.18
5 4800 3460 3690 134 60 7520 2148 119 16.0 1 2 180 202 0.15 0.13
6 4730 3020 3670 116 40 8640 1829 122 28.0 0 0 180 202 0.18 0.13
I 7 5460 3240 3460 100 40 8940 1728 191 14.0 0 2 160 202 0.18 0.14
8 4230 3450 3710 125 50 9190 1720 82 16.4 2 2 160 202 0.19 0.18
9 4810 4150 2710 162 20 8540 1692 106 16.2 2 2 160 202 0.14 0.17
10 5340 4980 3280 149 30 10340 2568 146 16.4 1 2 150 202 0.11 0.16
11 4000 3890 4280 175 60 9260 2468 223 12.4 1 2 150 202 0.15 0.16
I 12 4240 3820 3750 155 10 9340 2376 136 17.4 0 2 150 202 0.14 0.15
13 4800 4450 4140 140 70 1829 132 24,0 1 0 150 202 0.20 0.15
14 4480 4000 4040 143 90 8700 2048 125 17.6 1 1 150 202 0.18 0.16
15 3650 3070 3210 138 40 11980 1976 108 12.8 1 2 150 202 0.14 0.16
16 4110 2650 3990 145 30 8490 2108 128 17.0 1 2 150 202 0.17 0.17
I 17 4970 4190 3400 140 190 10410 2412 120 17.4 1 2 150 202 0.13 0.16
18 3560 3510 3990 155 40 10090 1896 134 20.0 1 2 150 202 0.19 0.16
19 4000 3450 3870 132 50 10820 2412 149 25.0 0 0 150 202 0.14 0.15
20 4030 3440 3890 128 230 9100 1984 154 22.0 0 1 160 202 0.17 0.16
21 3930 2730 3070 115 140 8770 2044 167 28.1 0 0 140 200 0.13 0.15
I 22 3590 3650 4300 136 100 7800 1940 113 24.7 1 2 150 202 0.20 0.17
23 4810 4090 4000 150 30 11040 2160 175 27.5 0 0 150 202 0.16 0.16
24 5370 4580 3030 109 20 7820 2280 105 22.0 1 2 150 202 0.12 0.16
25 3720 3300 3400 129 60 10030 1852 129 24.6 0 0 150 202 0.16 0.16
26 4200 3630 3550 104 20 7700 1824 102 20.1 2 2 150 202 0.17 0.16
I 27 4040 3320 3040 132 50 5200 1640 148 21.5 0 0 150 202 0.16 0.16
28 5020 3910 3650 115 60 9060 1668 129 24.0 1 2 130 202 0.19 0.16
29 6100 3800 4600 146 30 10060 2520 138 28.0 0 0 140 202 0.16 0.17
30 4370 4570 4650 135 30 9240 1780 175 14.0 0 2 150 202 0.24 0.19
31 5190 4670 4350 147 30 5500 1760 116 20.1 1 2 150 202 0.22 0.20
I AVG: 4547 3755 3588 132 57 8962 2038 137.7 19.9 1 1 156 202 0.16
MAX: 8120 4980 4850 175 230 11980 2568 223.0 28.1. 2 3 180 202 0.24
MIN: 3550 2650 0 0 0 5200 1640 82.0 10.8 0 0 130 200 0.00
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GROUNDWATER MONTHLY MONITORING:
RAINFALL DATA
uATE MAR. INCHES/iJAX
03/01/99 o.oo
03/02/99 o.oo
03/03/99 0.90
03/04/99 0.00
03/05/99 0.00
03/06/99 0.00
03/07/99 0.00
03/08/99 0.10
03/09/99 0.20
03/10/99 o.oo
03/11/99 o.oo
03/12/99 o.oo
03/13/99 0.40
03/14/99 0.60
03/15/99 0.00
03/16/99 o.oo
03/17/99 o.oo
03/18/99 0.00
03/19/99 0.00
03/20/99 0.70
03/21/99 0.20
03/22/99 o.oo
03/23/99 0.00
03/24/99 o.oo
03/25/99 0.00
03/26/99 0.10
03/27/99 0.00
03/28/99 0.00
03/29/99 o.oo
03/30/99 0.00
03/31/99 1.50
TOTAL 4.70
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MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
A'-'IIUN
DATE WELL# PROBLEM DATE ACTION
3/4/99 #1 LOW FLOW 3/4/99 REPLACED EXHUSTER
3/4/99 #2 LOW FLOW 3/4/99 ADJUSTED FLOAT
3/4/99 #3 LOW FLOW 3/4/99 CLEANED LINE & CHANGED BLADDER
3/4/99 #8 NO FLOW 3/4/99 REPLACED EXHUSTER
3/4/99 #9 LOW FLOW 3/4/99 CLEANED PROBES
3/11 /99 #3 LOW FLOW 3/11/99 CLEANED SCREEN
3/15/99 #4 LOW FLOW 3115/99 REPLACED EXHUSTER & METER
3/18/99 #4 LOW FLOW 3/18/99 REPLACED BLADDER
3/19/99 #3 NO FLOW 3/23/99 NEW PUMP & LINE
3/29/99 #8 LOW FLOW 03/29/99 ADJUSTED CONTROLS
3/29/99 #9 LOW FLOW 03/29/99 CLEANED PROBES
3/31/99 #4 LOW FLOW 03/31/99 INSTALLED WATER LINE.
MECHANIC
PHIL. P
PHIL. P
PHIL.P
PHIL.P
PHIL.P
PHILP
PHIL. P
PHIL. P
LYNB.
PHIL. P.
PHIL. P.
PHIL. P.
Well
OT-2R
OT-3
OT-4
OT-5
OT-6
OT-GA
OT-7
OT-8
Thermometer
Operational? ••
X
X
X
X
X
X
X
X
Monthly O&M Plan Checklist
HNA Holdings, Inc., Shelby, NC
Heat Lamp
Operational? ••
X
X
X
X
X
X
X
X
Other Operational Items/Comments
(** Temperature and Heat Lamp checks October thru April only)
Form Completed by: __________ T:..:O:.:.N.:..;Y:...;B::::R.:.:Yc:.A"-NT:..;._ ________ _
Oate: __________ 3"-'/--'1-'--/-'-99c.-________ _ - - - - - - - - - - - - - - - -·-- -
I
I INNER TIER
DAILY FLOW
I APRIL ' llil LI:1 1H ~ II:! 1H. II:2 1H lI:!l lI:ll
I 04101199 154 35 43 113 375 142 451 334 17
04102199 153 35 43 13 374 135 241 395 523
04/03199 147 34 42 0 394 120 238 424 535
04104199 151 35 43 0 410 123 238 388 542
I 04105199 146 34 42 69 401 120 219 333 532
04/06199 147 34 43 76 404 124 233 396 541
04107199 147 35 90 105 407 122 228 404 541
04108199 116 29 78 86 323 97 184 248 423
04109199 139 31 100 102 225 109 196 262 478
I 04110199 159 38 113 125 390 134 232 433 579
04111/99 137 32 100 113 340 113 203 410 491
04112199 145 34 110 125 373 121 225 448 531
04113/99 143 34 110 124 379 119 221 432 535
I 04114199 140 35 110 124 392 119 221 311 538
04115199 138 33 106 124 388 118 227 386 539
04116/99 115 28 91 99 315 95 177 280 430
04117199 136 6 102 100 281 104 173 267 464
04118199 141 0 108 121 293 119 215 187 527
I 04119/99 131 44 98 105 143 105 181 39 460
04120199 145 41 110 120 130 119 202 460 533
04121/99 135 4 103 110 266 115 186 486 501
04122199 134 0 103 114 282 114 189 593 514
I 04123199 141 0 108 113 290 114 188 412 532
04124199 139 0 109 114 284 116 179 525 536
04125199 141 0 138 113 287 115 194 543 546
04126199 141 46 78 111 272 115 185 556 568
04127199 137 46 105 110 280 115 167 555 565
I 04128/99 134 41 106 111 278 106 170 597 567
04129199 135 36 105 107 287 110 174 612 569
04130199 132 35 105 107 282 109 163 614 561
I AVG: 140 28 91 98 318 116 210 411 507
I TOTAL: 4199 835 2742 2954 9545 3487 6300 12330 15218
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INNER TIER COMBINED INFLUENT #2 ITCI
PAGE NO.1
APRIL.1999 I DATE: FLOW: PH: COD: TSS: TOC:
GPD pH ppm ppm ppm
04/01/99 1664 5.3 5320 4 1580 I 04/02/99 1912 5.4 7780 25
04/03/99 1934 5.4 4000 14
04/04/99 1930 5.4 6130 17 I 04/05/99 1896 5.3 5190 3
04/06/99 1998 5.4 4850 12
04/07/99 2079 5.4 5060 19
04/08/99 1584 5.4 4100 22 I 04/09/99 1642 5.4 5940 23
04/10/99 2203 5.4 3730 11
04/11/99 1939 5.3 3960 8 I 04/12/99 2112 5.4 5770 20
04/13/99 2097 5.4 4400 14
04/14/99 1990 5.4 4960 8 1610
04/15/99 2059 5.4 4830 5 I 04/16/99 1630 5.4 4690 5
04/17/99 1633 5.4 4330 11
04/18/99 1711 5.4 4840 5
04/19/99 1306 5.4 5600 11 I 04/20/99 1860 5.3 5770 12
04/21/99 1906 5.4 5430 15 1680
04/22/99 2046 5.4 4470 4
04/23/99 · 1898 5.4 5310 20 I 04/24/99 2002 5.3 5010 13
04/25/99 2077 5.3 5120 7
04/26/99 2072 5.4 4640 8 I 04/27/99 2080 5.3 4530 3
04/28/99 2110 5.3 5730 6 1570
04/29/99 2135 5.3 4890 10
04/30/99 2108 5.3 4290 16 I
AVG: 1920 5.4 5022 12 1610
MAX: 2203 5.4 7780 25 1680 I MIN: 1306 5.3 3730 3 1570
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I GROUNDWATER MONTHLY MONITORING:
INNER TIER EQUALIZATION TANK: ITEQT
I PAGE NO. 2
APRIL.1999
DATE: PH: COD: OT WATER ADDED '
pH ppm gal
I 04/01/99 7.5 3670
04/02/99 7.3 5950
04/03/99 7.2 5390
I 04/04/99 7.6 4960 375
04/05/99 7.5 5010
04/06/99 7.5 3780 450
04/07/99 7.5 4520 534
I 04/08/99 7.6 3530
04/09/99 7.4 4950
04/10/99 7.6 3930
I 04/11/99 7.5 4370
04/12/99 7.4 5260 563
04/13/99 7.6 3400 375
04/14/99 7.4 3140 563
I 04/15/99 7.4 4300 488
04/16/99 5.7 3660
04/17/99 7.2 3990
04/18/99 7.4 5220
I 04/19/99 7.4 3790
04/20/99 7.2 4390
04/21/99 7.2 5110
I 04/22/99 7.4 3200
04/23/99 7.3 4090 583
04/24/99 7.2 4290
04/25/99 7.2 4110
I 04/26/99 7.2 2590 563
04/27/99 7.4 3460 563
04/28/99 7.4 3940 375
04/29/99 7.4 3840 375
I 04/30/99 7.4 3620 488
AVG: 7.3 4182 484
I MAX: 7.6 5950 583
MIN: 5.7 2590 375
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.. GROUNDWATER MONTHLY MONITORING: I
AFTER PLATE SEPARATOR BEFORE SBR: SBRI
PAGE NO. 3 I APRIL.1999
DATE: PH: COD: TSS:
pH ppm ppm
04/01/99 I 04/02/99 7.0 5730 24
04/03/99 5.4 5260 24
04/04/99 5.4 5000 20 I 04/05/99 5.4 4400 16
04/06/99 6.0 3550 8
04/07/99 5.5 3400 16
04/08/99 I I 04/09/99 5.4 4760 8
04/10/99 6.1 3930 4
04/11/99 5.7 3690 8 I 04/12/99 6.1 3850 8
04/13/99 5.8 3880 4
04/14/99 5.8 3430 3
04/15/99 5.6 3270 9 I 04/16/99
04/17/99 . 5.5 3350 14
04/18/99
04/19/99 5.3 4300 8 I 04/20/99
04/21/99 5.3 4610 8
04/22199 5.6 4080 4 I 04/23/99 6.0 3420 40
04/24/99 7.0 3830 56
04/25/99 6.2 3330 36
04/26/99 6.0 3290 12 I 04/27/99 5.8 3820 8
04/28/99 5.8 2930 28
04/29/99 6.1 4200 8
04/30/99 6.1 4620 16 I
AVG: 5.8 3997 16
MAX: 7.0 5730 56 I MIN: 5.3 2930 3
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I GROUNDWATER MONTHLY MONITORING:
SBR MIXED LIQUOR: SBRML
I PAGE NO.4
APRIL.1999 SETT. SLUDGE 5/DAY
DATE: PH: NH3N: PO4: DO: MLSS: MLVSS: SOLIDS: WASTED F/M: F/M:
pH ppm ppm ppm ppm ppm ml/I gal ratio ratio
I 04/01/99 8.5 98 23.1 5.9 2108 150 202 0.00
04/02199 8.7 134 36.8 4.9 1812 150 0 0.28
04/03/99 8.6 134 1.0 6.4 1856 150 202 0.25
I 04/04/99 8.7 122 29.0 5.4 1880 150 202 0.24
04/05/99 8.8 95 21.0 6.6 1764 150 202 0.22 0.20
04/06/99 8.9 125· 16.0 6.2 1892 1492 150 202 0.17 0.23
04/07/99 8.8 109 20.0 6.8 2168 150 202 0.14 0.20
I 04/08/99 8.9 149 21.0 4.8 1804 150 202 0.00 0.15
04/09/99 9.0 100 27.6 6.9 1816 150 202 0.23 0.15
04/10/99 8.7 180 28.2 4.9 1728 170 202 0.20 0.15
I 04/11/99 8.9 120 13.0 5.6 1772 140 240 0.19 0.15
04/12199 8.8 82 16.8 5.0 1820 140 202 0.19 0.16
04/13/99 8.9 112 25.0 6.6 1796 1372 130 202 0.19 0.20
04/14/99 8.9 124 24.4 6.0 1724 130 202 0.18 0.19
I 04/15/99 8.9 199 16.4 7.7 1812 130 202 0.16 0.18
04/16/99 8.9 121 19.4 7.0 1732 130 202 0.00 0.14
04/17/99 9.0 140 21.0 6.1 2008 100 202 0.15 0.14
04/18/99 9.0 134 17.4 6.6 1456 100 202 0.00 0.10
I 04/19/99 9.0 138 10.0 8.3 1624 100 202 0.24 0.11
04/20/99 8.8 170 17.6 6.2 1684 1272 100 202 0.00 0.08
04/21/99 8.8 136 26.2 2.3 1752 100 135 0.23 0.12
04/22/99 8.2 135 31.6 2.8 1712 100 135 0.21 0.14
I 04/23/99 8.0 136 20.0 2.5 1516 100 100 0.20 0.18
04/24/99 8.0 114 23.6 2.1 1776 100 135 0.19 0.17
04/25/99 8.0 130 19.0 2.0 1568 100 135 0.19 0.21
I 04/26/99 8.0 120 13.7 1.6 1852 100 100 0.16 0.19
04/27/99 8.0 134 16.0 2.5 . 1724 1348 100 135 0.20 0.19
04/28/99 8.0 134 20.0 2.8 1492 100 135 0.17 0.18
04/29/99 8.0 42 17.2 1.9 1320 100 135 0.28 0.20
I 04/30/99 8.0 119 21.2 2.0 1572 100 100 0.26 0.21
AVG: 8.6 126 20 5 1751 1371 124 171 0.17 0.17
I MAX: 9.0 199 37 8 2168 1492 170 240 . 0.28 0.23
MIN: 8.0 42 1 2 1320 1272 100 0 0.00 0.08
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GROUNDWATER MONTHLY MONITORING: I
SBR EFFLUENT:(DECANT) #4 SBRE
PAGE NO. 5 I APRIL.1999 WAS. NH3N PHOS.
DATE: FLOW: COD: TSS: TSS ADDED: ADDED:
GPO ppm ppm ppm gal lbs
04/01/99 0 5820 2 2 I 04/02/99 1839 151 70 0 0
04/03/99 1805 140 90 10250 0 2
04/04/99 1820 130 60 9570 0 0 I 04/05/99 1869 121 40 7360 1 1
04/06/99 1875 169 20 4140 1 2
04/07/99 2153 145 40 9550 1 2
04/08/99 0 10200 0 0 I 04/09/99 1787 220 40 7140 1 0
04/10/99 2376 130 384 6870 0 0
04/11/99 1828 170 100 9820 0 1 I 04/12/99 2055 153 140 5150 2 2
04/13/99 2060 211 90 9830 1 2
04/14/99 2333 244 80 7790 1 1
04/15/99 1892 218 100 8050 0 2 I 04/16/99 0 9670 1 2
04/17/99 1965 209 140 7220 1 2
04/18/99 0 4540 1 2
04/19/99 2625 240 110 6690 1 2 I 04/20/99 0 3700 0 2
04/21/99 2813 215 60 8940 1 1
04/22/99 2720 188 10 2540 1 0 I 04/23/99 3083 166 100 8300 1 1
04/24/99 2257 171 90 8100 1 1
04/25/99 2033 174 60 10660 1 1
04/26/99 2226 173 40 9300 2 2 I 04/27/99 2079 192 30 10700 1 2
04/28/99 2345 105 110 8470 1 2
04/29/99 2244 190 50 10300 2 2
04/30/99 2311 211 100 11010 1 1 I
AVG: 1813 177 86 7989 1 1
MAX: 3083 244 384 11010 2 2 I MIN: 0 105 10 2540 0 0
• DID NOT PROCESS SBR.
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I GROUNDWATER MONTHLY MONITORING
INNER TIER CARBON FILTER EFFLUENT #8 ITEF
I PAGE NO. 7
APRIL.1999
DATE: PH: COD: TOG: TSS:
pH ppm ppm ppm
I 04/01/99
04/02/99
04/03/99
I 04/04/99
04/05/99
04/06/99
04/07/99 8.5 92 6 20
I 04/08/99
04/09/99
04/10/99
I 04/11/99
04/12/99
04/13/99
04/14/99 8.7 132 7
I 04/15/99
04/16/99
04/17/99
04/18/99
I 04/19/99
04/20/99
04/21/99 8.6 168 8
04/22/99
I 04/23/99
04/24/99
04/25/99
I 04/26/99
04/27/99
04/28/99 8.2 81 9
04/29/99
I 04/30/99
AVG: 8.5 118 8 20
I MAX: 8.7 168 9 20
MIN: 8.2 81 6 20
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DAILY REFERENCE SHEET: I
DATE: IT. EQ. PLT. DEC. DEC. WAS MIX MIX MIX NIT PHOS MIX F/M I APRIL. INF. TNK. SEP. LIQ LIQ LIQ ADD ADD LIQ WAS 5/DAY
mi CQO. CQO. CQO. CQO. :rs.s. .ns. MLll ' NII fttQS. ~ LBS. SEL ~ E1M AYSl.
1 5320 3670 5820 2108 98 23.1 2 2 150 202 0.00
2 7780 5950 5730 151 70 1812 134 36.8 0 0 150 0 0.28 I 3 4000 5390 5260 140 90 10250 1858 134 1.0 0 2 150 202 0.25
4 6130 4960 5000 130 60 9570 1880 122 29.0 0 0 150 202 0.24
5 5190 5010 4400 121 40 7360 1764 95 21.0 1 1 150 202 0.22 0.20
6 4850 3780 3550 169 20 4140 1892 125 16.0 1 2 150 202 0.17 0.23
7 5060 4520 3400 145 40 9550 2168 109 20.0 1 2 150 202 0.14 0.20 I 6 4100 3530 10200 1804 149 21.0 0 0 150 202 0.00 0.15
9 5940 4950 . 4760 220 40 7140 1816 100 27.6 1 0 150 202 0.23 0.15
10 3730 3930 3910 130 384 6870 1729 180 28.2 0 0 170 202 0.20 0.15
11 3960 4370 3690 170 100 9820 1772 120 13.0 0 1 140 240 0.19 0,15
12 5770 5260 3850 153 140 5150 1820 140 16.8 2 2 140 202 0.19 0.16 I 13 4400 3400 3860 211 90 8830 1796 112 25.0 1 2 130 202 0.19 0.20
14 4960 3140 3430 244 60 7790 1724 124 24.4 1 1 130 202 0.18 0.19
15 4830 4300 3270 218 100 8050 1812 199 18.4 0 2 130 202 0.18 0.18
16 4890 3660 9670 1732 121 19.4 1 2 130 202 0.00 0.14
17 4330 3990 3350 209 140 7220 2008 140 21.0 1 2 100 202 0.15 0.14 I 18 4840 5220 4540 1458 134 17.4 1 2 100 202 0.00 0.10
19 5600 3790 4300 240 110 6690 1624 138 10.0 1 2 100 202 0.24 0.11
20 5770 4390 3700 1684 170 17.6 0 2 100 202 0.00 0.08
21 5430 5110 4810 215 60 8940 1752 136 26.2 1 1 100 135 0.23 0.12
22 4470 3200 4080 188 10 2540 1712 135 31.6 1 0 100 135 0.21 0.14 I 23 5310 4090 3420 166 40 8300 1516 136 20.0 1 1 100 100 0.20 0,18
24 5010 4290 3830 171 90 8100 1776 114 23.6 1 1 100 135 0.19 0.17
25 5120 4110 3330 174 60 10660 1568 130 19.0 1 1 100 135 0.19 0.21
26 4840 2590 3290 173 40 9300 1852 120 13.7 2 2 100 100 0.16 0.19
27 4530 3460 3820 192 30 10700 1724 134 16.0 1 2 100 135 0.20 0.19 I 28 5730 3940 2930 105 110 8470 1492 134 20.0 1 2 100 135 0.17 0.18
29 4890 3840 4200 190 50 10300 1320 42 17.2 2 2 100 135 0.28 0.20
30 4290 3620 4620 211 100 11010 1572 119 21.2 1 1 100 100 0.26 0.21
AVG: 5022 4182 3643 171 81 7723 1751 128.1 20.4 1 1 124 171 0.17 I MAX: 7780 5950 5730 244 384 11010 2188 199.0 38.8 2 2 170 240 0.28
MIN: 3730 2590 0 0 0 0 1320 . 42.0 1.0 0 0 100 0 0.00
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GROUNDWATER MONTHLY MONITORING:
RAINFALL DATA
DATE APR. 1,.._HE:stDAY
04/01/99 0.00
04/02/99 o.oo
04/03/99 0.00
04/04/99 0.00
04/05/99 0.00
04/06/99 0.00
04/07/99 o.oo
04/08/99 0.10
04/09/99 o.oo
04/10/99 0.00
04/11/99 0.00
04/12/99 o.oo
04/13/99 0.00
04/14/99 0.00
04/15/99 0.30
04/16/99 0.00
04/17/99 o.oo
04/18/99 0.00
04/19/99 o.oo
04/20/99 0.00
04/21/99 o.oo
04/22/99 0.00
04/23/99 0.00
04/24/99 0.00
04/25/99 0.00
04/26/99 0.20
04/27/99 1.00
04/28/99 0.10
04/29/99 2.00
04/30/99 0.40
TOTAL 4.10
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
"" IIUN
DATE WELL# PROBLEM DATE ACTION
4/5/99 #4 LOW FLOW 4/5/99 REPLACED EXHUSTER & AIR LINES
4/8/99 #3 LOW FLOW 4/8/99 ADJUSTED CONTROLS
4/8/99 #4 LOW FLOW 4/8/99 ADJUSTED CONTROLS
4119/99 #2 NO FLOW 4/19/99 FREED CHECK VALVE IN PUMP
4/19/99 #8 LOW FLOW 4/19/99 REPLACED BLADDER &ALL LINES
4/26/99 #2 NO FLOW 4/26/99 ADJUSTED CONTROLS
MECHANIC
MAX&P.P.
MAX&P.P.
MAX&P.P.
MAX&P.P.
MAX&P.P.
L.B.
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- - - - - - - - - -·--· - - - - - - -
Well
OT-2R
OT-3
OT-4
OT-5
OT-6
OT-GA
OT-7
OT-8
Thermometer
Operational? **
X
X
X
X
X
X
X
X
Monthly O&M Plan Checklist
HNA Holdings, Inc., Shelby, NC
Heat Lamp
Operational? **
X
X
X
X
X
X
X
X
Other Operational Items/Comments
(** Temperature and Heat Lamp checks October thru April only)
Form Completed by: __________ T~O:.:Nc.Yc.B:ccR.cY.cA.c.NccT _________ _
Date: __________ _:;4/c.1:c./-=9-=9 __________ _
. Quarterly O&M Plan Checklist-HNA Holdings, lnc./Shelby, NC
Outer Tier Well
OT-ZR
OT-3
OT-4
OT-S
OT-6
OT-6A
OT-7
OT-8
·Ground-Water
Treatment Sys.
- - -
Open Sample
Port
X
X
X
X
X
X
X
X
Energize
AS Blower
Y-V-1008
-
Energize
Pump
X
X
X
X
X
X
X
X
Energize
Transfer Purrc,
Y..P-1007A
- -
Verify De~nerglze Close Sample
Discharge Pump Port
X X X
X X X
X X X
X X X
X X X
X X X
X X X
X X X
Energize Energize Energize
Transfer Pump Transfer Pump Transfer Pump
Y-P-1007B Y-P-1008A Y-P-10088
- - - -
Form Completed by: TONY BRYANT
Date: 4/1/99
Verify Heater Secure WeU
Operation Vault Comments
X X
X X
X X
X X·
X X
X X
X X
X X
Comments
- -- - - - - - -
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I May 1999 O&M Data
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I Kubal-Furr & Associates
I
I INNER TIER
DAILY FLOW
I MAY ' 19li 1I.:1 lI:Z lI:3. 1H 1H. II:6. II:I 1H. rut
I 05/02/00 123 34 101 100 269 106 146 599 541
05/02/99 123 30 92 86 250 98 131 530 495
05/03/99 128 36 98 83 257 102 7 550 464
05/04/99 137 35 104 92 277 114 0 638 594
05/05/99 136 31 107 94 296 114 92 662 603
I 05/06/99 138 34 107 94 307 116 154 670 611
05/07/99 131 34 102 91 295 109 148 614 593
05/08/99 103 24 80 71 225 84 116 492 451
05/09/99 124 8 99 67 286 94 119 555 534
I 05/10/99 134 37 104 75 318 118 143 634 608
05/11/99 108 36 84 61 253 89 120 516 502
05/12/99 125 6 98 59 280 95 127 541 548
05/13/99 134 0 107 68 314 113 154 645 660
05/14/99 133 52 112 76 308 111 144 636 658 I 05/15/99 100 33 72 59 240 86 104 489 525
05/16/99 126 43 99 61 290 96 119 553 556
05/17/99 134 38 107 71 319 112 141 633 680
05/18/99 133 34 173 160 328 113 141 633 722
I 05/19/99 133 32 116 90 322 113 138 513 704
05/20/99 102 20 89 72 247 100 106 59 543
05/21/99 122 0 105 84 294 94 113 252 541
05/22/99 136 0 110 97 327 112 136 385 695
I 05/23/99 129 0 106 103 313 108 132 166 614
05/24/99 122 0 104 106 308 112 126 212 643
05/25/99 122 40 108 109 304 112 135 685 649
05/26/99 94 33 90 86 240 86 105 0 484
05/27/99 114 7 95 93 278 98 115 524 514
I 05/28/99 119 0 107 102 303 114 131 508 548
05/29/99 118 50 106 105 291 147 131 507 493
05/30/99 122 43 107 107 275 105 129 500 434
05/31/99 125 39 106 107 271 104 132 482 394
I AVG: 123 26 103 88 287 106 120 496 568
TOTAL: 3828 809 3195 2729 8885 3275 3735 15383 17601
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INNER TIER COMBINED INFLUENT #2 ITCI
PAGE N0.1 I MAY.1999
DATE: FLOW: PH: COD: TSS: TOG:
GPO pH ppm ppm ppm
05/01/99 2019 5.3 4530 5 I 05/02/99 1835 5.4 4260 10
05/03/99 1725 5.4 4970 9
05/04/99 1991 5.4 4650 20 I 05/05/99 2135 5.3 4940 24 1210
05/06/99 2231 5.4 5430 7
05/07/99 2117 5.4 3180 6
05/08/99 1646 5.4 5260 8 I 05/09/99 1886 5.4 3420 5
05/10/99 2171 5.4 5360 9
05/11/99 1769 5.3 7600 7 I 05/12/99 1879 5.3 4940 10 1350
05/13/99 2195 5.3 4600 8
05/14/99 2230 5.3 4940 7
05/15/99 1708 5.3 4770 6 I 05/16/99 1943 5.2 4860 5
05/17/99 2235 5.2 3930 2
05/18/99 2437 5.3 3390 10
05/19/99 2161 5.3 3790 16 1310 I 05/20/99 1338 5.3 4980 14
05/21/99 1605 5.3 4020 13
05/22/99 1998 5.3 5300 7 I 05/23/99 1671 5.3 3360 6
05/24/99 · 1733 5.2 4510 9
05/25/99 2264 5.2 4510 9
05/26/99 1218 5.2 3860 4 1450 I 05/27/99 1838 5.1 3820 7
05/28/99 1932 5.3 4230 12
05/29/99 1948 5.3 3750 6
_05/30/99 1822 5.3 4240 4 I 05/31/99 1760 5.2 4530 1
AVG: 1917 5.3 4514 9 1330
MAX: 2437 5.4 7600 24 1450 I MIN: 1218 5.1 3180 1 1210
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I GROUNDWATER MONTHLY MONITORING:
INNER TIER EQUALIZATION TANK ITEQT
PAGE NO. 2
I MAY.1999
DATE: PH: COD: OT WATER ADDED '
pH ppm gal
I 05/01/99 7.2 3640
05/02/99 7.2 3090
05/03/99 7.2 2540
I 05/04/99 7.2 3780 375
05/05/99 7.2 3240 189
05/06/99 7.5 3340 94
05/07/99 7.4 3690 375
I 05/08/99 7.3 4290
05/09/99 7.4 3620
05/10/99 7.3 4710 488
I 05/11/99 7.6 3640
05/12/99 7.2 4770
05/13/99 7.5 4720
05/14/99 7.4 4420 375
I 05/15/99 7.4 4030
05/16/99 7.3 4340
05/17/99 7.1 3910 338
05/18/99 7.2 3490 450
I 05/19/99 7.7 3870 375
05/20/99 7.4 3440
05/21/99 7.3 2990
05/22/99 7.2 3630
I 05/23/99 7.3 2840
05/24/99 7.2 3560
05/25/99 7.3 3940 189
I 05/26/99 7.3 3650 375
05/27/99 7.4 3530
05/28/99 7.4 3040
05/29/99 7.4 3580
I 05/30/99 7.4 3850
05/31/99 7.4 3190
AVG: 7.3 3689 329
I MAX: 7.7 4770 488
MIN: 7.1 2540 94
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GROUNDWATER MONTHLY MONITORING: I AFTER PLATE SEPARATOR BEFORE SBR: SBRI
PAGE NO. 3 I , MAY.1999
DATE: PH: COD: TSS:
pH ppm ppm
05/01/99 6.5 2480 20 I 05/02/99
05/03/99 6.3 2540 16
05/04/99 6.0 3760 4 I 05/05/99 6.6 2360 64
05/06/99 6.4 2620 4
05/07/99 6.4 2850 4
05/08/99 I 05/09/99 6.2 2700 44
05/10/99 6.3 4100 16
05/11/99 I 05/12/99 6.3 3940 32
05/13/99 6.5 3600 28
05/14/99 5.5 2910 12
05/15/99 I 05/16/99 6.6 3710 32
05/17/99 5.6 4130 3
05/18/99 5.8 4080 8
05/19/99 5.9 3360 20 I 05/20/99
05/21/99 5.6 2800 8
05/22/99 6.2 3790 48 I 05/23/99
05/24/99 5.6 3250 8
05/25/99 5.7 3990 32
05/26/99 5.8 3180 4 I 05/27/99 5.8 3130 20
05/28/99 6.1 3700 16
05/29/99 6.4 2880 12
05/30/99 5.6 3260 8 I 05/31/99 6.4 2600 12
AVG: 6.1 3269 19
MAX: 6.6 4130 64 I MIN: 5.5 2360 3
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I GROUNDWATER MONTHLY MONITORING:
SBR MIXED LIQUOR: SBRML
PAGE NO. 4 I MAY.1999 SETT. SLUDGE 5/DAY
DATE: PH: NH3N: PO4: DO: MLSS: MLVSS: SOLIDS: WASTED F/M: F/M:
pH ppm ppm ppm ppm ppm ml/I gal ratio ratio
I 05/01/99 8.0 194 27.0 2.6 1664 120 162 0.13
05/02/99 8.1 111 13.6 2.6 1752 100 0 0.00
05/03/99 8.0 134 25.4 2.5 1252 100 202 0.18
I 05/04/99 7.9 105 10.5 1.6 2004 1560 100 202 0.17
05/05/99 8.0 130 14.4 2.0 1568 100 202 0.13 0.12
05/06/99 8.0 141 15.0 2.1 1880 100 102 0.12 0.12
05/07/99 8.0 122 21.0 2.0 1820 100 189 0.14 0.15
I 05/08/99 8.0 118 19.0 1.8 1720 120 162 0.00 0.11
05/09/99 8.0 147 18.5 2.3 1516 100 150 0.16 0.11
05/10/99 8.0 113 14.0 2.4 1572 100 148 0.23 0.13
I 05/11/99 8.0 107 12.0 2.6 1600 100 135 0.00 0.11
05/12/99 8.0 134 33.0 2.6 1452 100 148 0.24 0.13
05/13/99 8.0 145 14.6 2.2 1572 50 70 0.20 0.17
05/14/99 8.0 103 33.2 2.6 1640 100 81 0.16 0.17
I 05/15/99 8.0 85 21.0 2.1 1560 100 81 0.00 0.12
05/16/99 8.0 92 20.0 1.9 1640 100 81 0.20 0.16
05/17/99 7.9 104 8.5 2.0 1504 100 102 0.24 0.16
05/18/99 7.9 128 10.0 1.9 1344 1076 100 102 0.27 0.17
I 05/19/99 8.0 88 13.6 2.5 1560 100 102 0.19 0.18
05/20/99 8.0 130 16.2 2.1 1632 100 102 0.00 0.18
05/21/99 8.0 146 22.6 2.4 1612 100 102 0.15 0.17
05/22/99 8.0 165 21.0 2.3 1532 100 100 0.22 0.17
I 05/23/99 8.0 171 14.2 2.4 1280 100 0 0.00 0.11
05/24/99 8.0 143 22.6 1.7 1828 100 102 0.16 0.11
05/25/99 8.0 148 11.0 2.1 1504 1208 100 102 0.24 0.15
I 05/26/99 8.0 104 13.2 2.4 1332 100 102 0.21 0.17
05/27/99 8.0 140 18.0 0.7 1792 100 102 0.16 0.15
05/28/99 8.0 123 17.6 2.0 1936 100 102 0.17 0.19
05/29/99 8.0 133 19.3 2.1 1532 100 102 0.17 0.19
I 05/30/99 8.0 140 22.6 2.2 1672 100 102 0.17 0.18
05/31/99 8.0 137 22.8 2.1 1224 100 102 0.19 0.17
AVG: 8.0 128 18 2 1597 1281 100 114 0.15 0.15
I MAX: 8.1 194 33 3 2004 1560 120 202 0.27 0.19
MIN: 7.9 85 9 1 1224 1076 50 0 0.00 0.11
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GROUNDWATER MONTHLY MONITORING: I
SBR EFFLUENT:(DECANT) #4 SBRE
PAGE NO. 5 I MAY.1999 WAS. NH3N PHOS.
DATE: FLOW: COD: TSS: TSS P.DDED: ADDED:
GPD ppm ppm ppm gal lbs
05/01/99 2404 206 50 11460 0 0 I 05/02/99 0 1 1
05/03/99 2369 220 60 10020 1 1
05/04/99 3000 215 10 10050 1 1 I 05/05/99 2588 215 110 2820 1 2
05/06/99 2700 253 10 11180 0 2
05/07/99 2481 220 60 11360 1 1 I 05/08/99 0 1 1
05/09/99 2003 211 140 11100 0 0
05/10/99 2756 212 70 10150 1 1
05/11/99 0 11010 1 1 I 05/12/99 2291 220 100 10830 0 0
05/13/99 2832 173 80 10370 0 0
05/14/99 2375 187 100 14620 0 0
05/15/99 0 6100 1 0 I 05/16/99 2782 190 50 10900 1 0
05/17/99 3000 216 100 10660 1 2
05/18/99 2270 195 90 4390 1 2
05/19/99 2358 196 100 9990 2 2 I 05/20/99 0 11400 1 2
05/21/99 2829 180 40 11000 0 0
05/22/99 2492 161 100 11140 0 0 I 05/23/99 0 1 1
05/24/99 2539 171 10 10800 0 0
05/25/99 2499 125 80 7500 0 2
05/26/99 2156 149 20 4000 1 2 I 05/27/99 1875 135 40 3180 1 2
05/28/99 2536 124 40 6380 1 2
05/29/99 2540 137 30 4150 1 2
05/30/99 2527 135 10 5550 1 2 I 05/31/99 2390 137 330 12910 1.0 2.0
AVG: 2019 183 73 9108 1 1
MAX: 3000 253 330 14620 2 2 I MIN: 0 124 10 2820 0 0 • DID NOT PROCESS SBR.
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I GROUNDWATER MONTHLY MONITORING
INNER TIER CARBON FILTER EFFLUENT #8 ITEF
I PAGE NO. 7
MAY.1999
DATE: PH: COD: TOC: TSS: ' pH ppm ppm ppm
I 05/01/99
05/02/99
05/03/99
I 05/04/99
05/05/99 8.2 161 8 140
05/06/99
05/07/99
I 05/08/99
05/09/99
05/10/99
I 05/11/99
05/12/99
05/13/99
05/14/99
I 05/15/99
05/16/99
05/17/99
05/18/99
I 05/19/99 8.2 174 10
05/20/99
05/21/99
05/22/99 I 05/23/99
05/24/99
05/25/99
I 05/26/99 8.1 135 9
05/27/99
05/28/99
05/29/99
I 05/30/99
05/31/99
AVG: 8.2 157 9 140
I MAX: 8.2 174 10 140
MIN: 8.1 135 8 140
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I DAILY REFERENCE SHEET:
DATE: IT. EQ. PLT. DEC. DEC. WAS MIX MIX MIX NIT PHOS MIX F/M I MAY INF. TNK. SEP. LIQ LIQ LIQ ADD ADD LIQ WAS 5/DAY
.1lli CQD. CQD. CQD. CQD. ISs. .lli MLSll.' till eH.QS. GALS. LB.S. s.EL GALS. ELM Al/SJ..
1 4530 3640 2480 206 50 11460 1664 194 27.0 0 0 120 162 0.13 I 2 4260 3090 1752 111 13.6 1 1 100 0 · 0.00
3 4970 4520 2540 220 60 10020 1252 134 25.4 1 1 100 202 0.18
4 4650 3780 3760 215 10 10050 2004 105 10.5 1 1 100 202 0.17
5 4960 3240 2360 215 110 2820 1568 130 14.4 1 2 100 202 0.13 0.12
6 5430 3340 2620 253 10 11180 1880 141 15.0 0 2 100 102 0.12 0.12 I 7 3180 3690 2850 220 60 11360 1820 122 21.0 1 1 100 189 0.14 0.15
8 5260 4290 1720 118 19.0 1 1 120 162 0.00 0.11
9 3420 3620 2700 211 140 11100 1516 147 18.5 0 0 100 150 0.16 0.11
10 5360 4710 4100 212 70 10150 15n 113 14.0 1 1 100 148 0.23 0.13
11 7600 3640 11010 1600 107 12.0 1 1 100 135 0.00 0.11
12 4940 4770 3840 220 100 10830 1452 134 33.0 0 0 100 148 0.24 0.13 I 13 4600 4720 3600 173 BO 10370 1572 145 14.6 0 0 50 70 0.20 0.17
14 4940 4420 2910 187 100 14620 1640 103 33.2 0 0 100 81 0.16 0.17
15 4770 4030 6100 1560 85 21.0 1 0 100 81 0.00 0.12
16 4860 4340 3710 190 50 10900 1640 92 20.0 1 0 100 81 0.20 0.16
17 3930 3910 4130 216 100 10660 1504 104 8.5 1 2 100 102 0.24 0.16 I 18 3390 3490 4080 195 100 4390 1344 128 10.0 1 2 100 102 0.27 0,17
19 3790 3870 3360 196 100 9990 1560 68 13.8 2 2 100 102 0.19 0.18
20 4980 3440 11400 1632 130 16.2 1 2 100 102 0.00 0.18
21 4020 2990 2800 180 40 11000 1612 146 22.8 0 0 100 102 0.15 0.17
22 5300 3830 3790 161 100 11140 1532 165 21.0 0 0 100 100 0.22 0.17 I 23 3360 2840 1280 171 14.2 1 1 100 0 0.00 0.11
24 4510 3560 3250 171 100 10800 1828 143 22.6 0 0 100 102 0.16 0.11
I
25 4510 3940 3990 125 80 7500 1504 148 11.0 0 2 100 102 0.24 0.15
26 3860 3650 3180 149 20 4000 1332 104 13.2 1 2 100 102 0.21 0.17
27 3620 3530 3130 135 40 3180 1792 140 18.0 1 2 100 102 0.16 0.15 I 28 4230 3040 3700 124 40 6380 1936 123 17.6 1 2 100 102 0.17 0.19
29 3750 3580 2880 137 30 4150 1532 133 19.3 1 2 100 102 0.17 0.19
30 4240 3850 3260 135 10 5550 16n 140 22.6 1 2 100 102 0.17 0.18
31 4530 3190 2600 132 30 12910 1224 137 22.8 1 2 100 102 0.19 0.17
AVG: 4515 3753 3143 176 63 6794 1597 126.4 18.2 1 1 100 114 0.15 0.14 I MAX: 7600 4770 4130 253 140 _14620 2004 194.0 33.2 2 2 120 202. 0.27 0.18
MIN: 3180 2940 0 0 0 0 1224 85.0 8.5 0 0 50 0 0.00 0.12
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GROUNDWATER MONTHLY MONITORING:
RAINFALL DATA
MAY
DATE T ·~ ;/DAY
05/01/99 0.00
05/02/99 0.00
05/03/99 0.00
05/04/99 o.oo
05/05/99 0.20
05/06/99 0.10
05/07/99 0.20
05/08/99 0.00
05/09/99 0.00
05/10/99 0.00
05/11/99 0.00
05/12/99 o.oo
05/13/99 0.60
05/14/99 0.00
05/15/99 0.00
05/16/99 o.oo
05/17/99 0.00
05/18/99 2.30
05/19/99 0.00
05/20/99 o.oo
05/21/99 o.oo
05/22/99 0.00
05/23/99 0.00
05/24/99 0.00
05/25/99 0.10
05/26/99 0.30
05/27/99 0.00
05/28/99 o.oo
05/29/99 o.oo
05/30/99 0.00
05/31/99 0.00
TOTAL 3.80
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
'"' IIUN
DATE WELL# PROBLEM DATE ACTION
5/21/99 #2 LOWFLOIW 5/24/99 CLEANED & RESTARTED
5/26/99 #8 LOW FLOW 5126/99 REPLACED PUMP
MECHANIC
L.B.
L.B.
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I INNER TIER
DAILY FLOW
I JUNE ' 1m II:1 11:2 I.H 1H 1H. 1H lI:Z. 1H. II:i
I 06/01/99 103 28 85 86 216 82 104 331 217
06/02/99 127 25 96 97 245 101 105 405 0
06/03/99 132 35 103 103 280 95 122 452 7
06/04/99 131 30 105 103 273 105 122 465 356
I 06/05/99 129 28 103 102 264 135 119 462 477
06/06/99 130 28 101 102 256 150 117 457 457
06/07/99 106 24 88 87 221 58 97 388 356
06/08/99 120 31 93 60 244 46 101 399 141
06/09/99 120 29 105 73 275 60 117 445 115
I 06/10/99 119 28 102 71 282 51 115 452 111
06/11/99 115 25 93 75 301 43 100 421 4
06/12/99 117 29 103 69 338 42 125 458 0
06/13/99 117 28 103 69 339 59 115 458 0
I 06/14/99 119 13 102 60 374 43 114 457 390
06/15/99 111 22 92 63 252 41 106 413 530
06/16/99 113 0 89 65 277 41 104 391 512
06/17/99 119 46 99 70 306 48 119 447 12
06/18/99 122 37 99 73 299 49 117 455 588
I 06/19/99 117 34 86 72 295 47 118 450 688
06/20/99 115 30 75 75 303 45 121 443 683
06/21/99 59 15 30 41 156 23 64 222 355
06/22/99 110 35 74 62 265 37 95 381 3
I 06/23/99 121 25 39 70 297 41 123 457 498
06/24/99 116 33 10 66 284 41 110 459 705
06/25/99 117 29 1 191 284 43 99 456 699
06/26/99 119 26 0 71 283 43 98 388 698
06/27/99 113 28 0 65 284 44 97 383 675
I 06/28/99 10 25 52 55 241 38 81 405 574
06/29/99 6 30 39 61 282 41 85 460 605
06/30/99 0 27 7 66 289 48 95 475 678
I AVG: 105 27 72 77 277 58 107 424 371
TOTAL: 3153 823 2174 2323 8303 1740 3203 12715 11134
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INNER TIER COMBINED INFLUENT #2 ITCI
PAGE NO.1 I JUNE.1999
DATE: FLOW: PH: COD: TSS: TOC:
GPD pH ppm ppm ppm
06/01/99 1252 5.2 3040 6 I 06/02/99 1201 5.2 4720 15 1580
06/03/99 1329 5.2 5000 7
06/04/99 1690 5.2 8210 12 I 06/05/99 1819 5.2 4760 9
06/06/99 1798 5.2 4910 7
06/07/99 1425 5.2 3780 4 I 06/08/99 1235 5.3 4920 13 1450
06/09/99 1339 5.3 4270 4
06/10/99 1331 5.2 5780 2
06/11/99 1177 5.2 5080 5 I 06/12/99 1279 5.1 7000 10
06/13/99 1288 5.2 6840 10
06/14/99 1672 5.2 6170 4
06/15/99 1630 5.2 3670 3 I 06/16/99 1592 5.2 4760 8 1450
06/17/99 1266 5.3 4000 4
06/18/99 1839 5.2 6430 10
06/19/99 1907 5.2 4100 14 I 06/20/99 1890 5.2 3800 6
06/21/99 965 5.2 4150 1
06/22/99 1062 5.2 4050 10 I 06/23/99 1671 5.2 6650 16
06/24/99 1824 5.2 3180 4 1330
06/25/99 1919 5.4 3670 10
06/26/99 1724 5.4 2690 10 I 06/27/99 1669 5.2 3650 9
06/28/99 1481 5.2 3990 8
06/29/99 1609 5.3 3820 7
06/30/99 1685 5.4 3700 10 1010 I
AVG: 1519 5.2 4693 8 1364
MAX: 1919 5.4 8210 16 1580 I MIN: 965 5.1 2690 1 1010
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I GROUNDWATER MONTHLY MONITORING:
INNER TIER EQUALIZATION TANK: ITEQT
I PAGE NO. 2
JUNE.1999
DATE: PH: COD: OT WATER ADDED '
pH ppm gal
I 06/01/99 7.4 3400
06/02/99 7.4 3950
06/03/99 7.4 4160 450
I 06/04/99 7.4 5770
06/05/99 7.5 5350
06/06/99 7.7 4980
I 06/07/99 8.4 3780
06/08/99 8.4 3900
06/09/99 8.4 3960
06/10/99 7.4 4430
I 06/11/99 7.4 5740
06/12/99 7.4 6080 563
06/13/99 7.5 4830
06/14/99 7.5 5030
I 06/15/99 7.7 4730
06/16/99 7.2 4300
06/17/99 7.4 4600 56
06/18/99 7.4 4840
I 06/19/99 7.3 4230
06/20/99 7.3 3980 375
06/21/99 7.4 3700 563
I 06/22199 7.6 3160
. 06/23/99 7.5 3860
06/24/99 7.2 4630
06/25/99 7.5 3480 563
I 06/26/99 7.6 3350 563
06/27/99 7.6 2410
06/28/99 7.6 3570
06/29/99 7.5 3330
I 06/30/99 7.5 3740
AVG: 7.6 4242 448
I MAX: 8.4 6080 563
MIN: 7.2 2410 56
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GROUNDWATER MONTHLY MONITORING: I
AFTER PLATE SEPARATOR BEFORE SBR: SBRI
PAGE NO. 3 I , "•JUNE.1999
DATE: PH: COD: TSS:
pH ppm ppm
06/01/99 I 06/02/99 6.2 3100 12
06/03/99 5.6 3440 4
06/04/99 I 06/05/99 6.7 4910 28
06/06/99 6.0 4970 20
06/07/99 I 06/08/99 5.4 4140 4
06/09/99 5.7 4170 12
06/10/99
06/11/99 5.8 5470 20 I 06/12/99 6.2 4810 20
06/13/99
06/14/99 5.3 3800 12
06/15/99 I 06/16/99 5.8 5550 16
06/17/99 5.4 4570 4
06/18/99
06/19/99 6.4 4480 24 I 06/20/99 6.4 3900 24
06/21/99
06/22199 5.9 3840 28 I 06/23/99
06/24/99 5.4 3250 4
06/25/99 5.5 4280 28
06/26/99 5.7 3250 16 I 06/27/99 6.0 2440 40
06/28/99
06/29/99 5.4 2710 8
06/30/99 6.1 2560 4 I
AVG: 5.8 3982 16 I MAX: 6.7 5550 40
MIN: 5.3 2440 4
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I GROUNDWATER MONTHLY MONITORING:
SBR MIXED LIQUOR: SBRML
PAGE NO. 4
I JUNE.1999 SETT. SLUDGE 5/DAY
DATE: PH: NH3N: PO4: DO: MLSS: MLVSS: SOLIDS: WASTED F/M: F/M:
pH ppm ppm ppm ppm ppm ml/I gal ratio ratio
I 06/01/99 8.0 169 16.0 2.2 1360 1000 100 142 0.00
06/02/99 8.0 170 32.4 · 2.2 1520 100 142 0.18
06/03/99 8.0 137 32.0 1.9 1688 100 142 0.18
I 06/04/99 8.0 136 29.6 2.1 1632 100 142 0.00
06/05/99 8.0 124 28.4 1.5 1500 100 142 0.29 0.13
06/06/99 8.0 126 24.0 1.8 1408 100 142 0.31 0.19
06/07/99 8.1 172 17.2 1.9 1516 100 142 0.00 0.16
I 06/08/99 8.0 141 8.0 1.8 1456 1080 100 142 0.25 0.17
06/09/99 8.1 122 14.0 1.7 1336 100 142 0.28 0.23
06/10/99 8.0 122 32.0 1.6 1308 100 142 0.00 0.17
06/11/99 8.1 112 22.4 1.9 1180 100 142 0.41 0.19
I 06/12/99 8.1 101 37.2 1.1 1360 100 142 0.31 0.25
06/13/99 8.2 109 13.2 1.2 1324 100 108 0.00 0.20
06/14/99 8.1 130 31.9 1.7 1200 100 108 0.28 0.20
I 06/15/99 8.1 124 25.7 1.5 1276 1000 100 108 0.00 0.20
06/16/99 8.1 115 24.8 1.7 1252 100 108 0.39 0.20
06/17/99 7.9 106 15.3 1.6 1280 100 108 0.32 0.20
06/18/99 8.1 101 22.8 2.0 1268 100 108 0.00 0.20
I 06/19/99 8.2 110 16.0 2.0 1280 100 108 0.31 0.20
06/20/99 8.1 105 17.0 1.6 1732 100 108 0.20 0.24
06/21/99 8.1 101 20.4 2.4 1364 100 108 0.00 0.17
06/22/99 8.1 110 29.0 1.8 1272 1020 100 108 0.27 0.16
I 06/23/99 8.1 90 10.0 2.3 1748 100 108 0.00 0.16
06/24/99 8.1 100 21.8 2.1 1312 70 108 0.22 0.14
06/25/99 8.1 106 19.2 1.6 1416 100 108 0.27 0.15
I 06/26/99 8.2 100 8.0 1.6 1296 150 40 0.22 0.20
06/27/99 8.1 134 20.6 2.1 1528 140 0 0.14 0.17
06/28/99 8.1 100 10.4 1.7 1380 1080 140 61 0.00 0.17
06/29/99 8.1 129 15.0 2.4 1356 150 61 0.18 0.16
I 06/30/99 8.1 102 28.0 1.5 1332. 150 61 0.17 0.14
AVG: 8.1 120 21 2 1396 1036 107 111 0.17 0.18
I MAX: 8.2 172 37 2 1748 1080 150 142 0.41 0.25
MIN: 7.9 90 8 1 1180 1000 70 0 0.00 0.13
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GROUNDWATER MONTHLY MONITORING: I
SBR EFFLUENT:(DECANT) #4 SBRE
PAGE NO. 5 I JUNE.1999 WAS. NH3N PHOS.
DATE: FLOW: COD: TSS: TSS ADDED: ADDED:
GPO ppm ppm ppm gal lbs
06/01/99 0 2620 1 2 I 06/02/99 2013 190 10 3110 0 0
06/03/99 2250 166 10 2050 0 0
06/04/99 0 3140 0 0 I 06/05/99 1889 172 60 8620 1 0
06/06/99 2348 158 70 10000 1 0
06/07/99 0 9660 0 0 I 06/08/99 2204 186 60 9950 0 2
06/09/99 2334 209 40 10480 0 2
06/10/99 0 10190 0 0
06/11/99 2073 181 90 7540 1 2 I 06/12/99 2354 192 90 8000 1 0
06/13/99 0 10800 1 2
06/14/99 2046 229 30 7340 0 0
06/15/99 0 7520 0 0 I 06/16/99 1980 200 50 7440 0 0
06/17/99 2318 198 20 7500 1 2
06/18/99 0 8380 0 0
06/19/99 2111 160 30 8250 1 2 I 06/20/99 2412 110 40 8190 1 2
06/21/99 0 9180 0 0
06/22/99 1972 109 24 8060 0 0 I 06/23/99 0. 7850 1 2.
06/24/99 2625 142 28 8800 1 ·2
06/25/99 2602 149 52 970 0 0
06/26/99 2336 147 40 9930 1 2 I 06/27/99 2455 148 56 0 0
06/28/99 0 9530 1 2
06/29/99 2216 136 30 7780 0 2
06/30/99 2392 117 40 6820 0 0 I
AVG: 1498 165 44 7576 0 1
MAX: 2625 229 90 10800 1 2 I MIN: 0 109 10 970 0 0 • DID NOT PROCESS SBR.
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I GROUNDWATER MONTHLY MONITORING
INNER TIER CARBON FILTER EFFLUENT #8ITEF
I PAGE NO. 7
JUNE.1999 ,. ,,
DATE: PH: COD: TOC: TSS: '
pH ppm ppm ppm
I 06/01/99
06/02/99 8.1 182 9 10
06/03/99
I 06/04/99
06/05/99
06/06/99
I 06/07/99
06/08/99 8.0 180 10
06/09/99
06/10/99
I 06/11/99
06/12/99
06/13/99
06/14/99
I 06/15/99
06/16/99 8.0 182 11
06/17/99
06/18/99
I 06/19/99
06/20/99
06/21/99
I 06/22/99
06/23/99
06/24/99 8.0 127 9
06/25/99
I 06/26/99
06/27/99
06/28/99
06/29/99
I 06/30/99 8.2 93 8
AVG: 8.1 153 9 10
I MAX: 8.2 182 11 10
MIN: 8.0 93 8 10
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DAILY REFERENCE SHEET: I
DATE: IT. EQ. PLT. DEC. DEC. WAS MIX MIX MIX NIT PHOS MIX F/M I JUNE INF. TNK. SEP. LIQ LIQ LIQ ADD ADD LIQ WAS 5/DAY
llli @o. @o. @o. @o. ~ ~ ~· NII e!:IQS. GALS. LBS. SET. GALS. ElM AY!J.,
1 3040 3400 2620 1360 169 16.0 1 2 100 142 0.00
2 4720 3950 3100 190 10 3110 1520 170 32.4 0 0 100 142 0.18 I 3 5000 4160 3440 168 10 2050 1688 137 32.0 0 0 100 142 0.18
4 8210 5770 1632 136 29.6 0 0 100 142 0.00
5 4760 5350 4910 172 60 8620 1500 124 28.4 1 0 100 142 0.29 0.13
6 4910 4980 4970 158 70 10000 1408 126 24.0 1 0 100 142 0.31 0.19
7 3780 3780 9680 1516 172 17.2 0 0 100 142 0.00 0.16 I 6 4920 3900 4140 166 60 9950 1456 141 8.0 0 2 100 142 0.25 0.17
9 4270 3960 4170 209 40 10480 1336 122 14.0 0 2 100 142 0.26 0.23
10 5780 4430 10190 1308 122 32.0 0 0 100 142 0.00 0.17 ·
11 5080 5740 5470 161 90 7540 1180 112 22.4 1 2 1()() 142 0.41 0.19
12 7000 6080 4810 192 90 8000 1360 101 37.2 1 0 100 142 0.31 0.25 I 13 6840 4830 10800 1324 109 13.2 1 2 100 108 0.00 0.20
14 6170 5030 3600 229 30 7340 1200 130 31.9 0 0 100 106 0.28 0.20
15 3670 4730 7520 1276 124 '25.7 0 0 100 108 0.00 0.20
16 4760 4300 5550 200 50 7440 1252 115 24.8 0 0 100 108 0.39 0.20
17 4000 4800 4570 196 20 7500 1280 106 15.3 1 2 100 106 0.32 0.20 I 18 6430 4840 8360 1268 101 22.8 0 0 100 108 0.00 0.20
19 4100 4230 4480 160 30 6250 1280 110 16.0 1 2 100 108 0.31 0.20
20 3800 3980 3900 110 40 8190 1732 105 17.0 1 2 100 106 0.20 0.24
21 4150 3700 9180 1364 101 20.4 0 0 100 106 0.00 0.17
22 4050 3160 3840 109 24 8060 1272 110 29.0 0 0 100 106 0.27 0.16 I 23 6650 3860 7650 1748 90 10,0 1 2 100 106 0.00 0.16
24 3180 4630 3250 142 28 8800 1312 100 21.8 1 2 70 106 0.22 0.14
'25 3870 3480 4280 149 52 970 1416 106 19.2 0 0 100 108 0.27 0.15
26 2960 3350 3250 147 40 9930 1296 100 8.0 1 2 100 40 0.22 0.20
27. 3650 2410 2440 148 56 1528 134 20.8 0 0 140 0 0.14 0.17 I 28 3990 3570 9530 1360 100 10.4 1 2 140 61 0.00 0,17
29 3820 3330 2710 136 30 7780 1356 129 15.0 0 2 150 61 0.18 0.18
30 3700 3740 '2560 117 40 6820 1332 102 18.0 0 0 150 61 0.17 0.14
AVG: 4702 4242 3792 157 41 7734 1396 120.1 21.1 0 1 105 111 0.17 0.10 I MAX: 8210 6080 5550 · 229 90 10800 1748 172.0 37.2 1 2 150 142 0.41 0.15
MIN: 2960 2410 0 0 0 970 1160 90.0 8.0 0 0 70 0 0.00 0.12
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GROUNDWATER MONTHLY MONITORING:
RAINFALL DATA
• .'DAY
06/01/99 0.00
06/02/99 1.50
06/03/99 0.20
06/04/99 0.00
06/05/99 0.00
06/06/99 0.00
06/07/99 0.00
06/08/99 0.00
06/09/99 0.00
06/10/99 0.90
06/11/99 o.oo
06/12/99 0.00
06/13/99 0.00
06/14/99 0.20
06/15/99 0.30
06/16/99 1.70
06/17/99 0.00
06/18/99 0.00
06/19/99 0.00
06/20/99 0.00
06/21/99 0.00
06/22/99 0.00
06/23/99 0.00
06/24/99 0.40
06/25/99 2.40
06/26/99 o.oo
06/27/99 o.oo
06/28/99 0.00
06/29/99 0.10
06/30/99 0.00
0.00
TOTAL 7.70
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
,..v l,v,.
DATE WELL# PROBLEM DATE ACTION
6/1/99 #8 LOW FLOW 6/1/99 CHANGED METER
6/1/99 #9 LOW FLOW 6/1/99 CHANGED METER
6/14/99 #4 LOW FLOW 6/14/99 ADJ. CONTROLS
6/14/99 #6 LOW FLOW 6/14/99 ADJ. CONTROLS
6/14/99 #9 NO FLOW 6/14/99 ELECTRICAL
6/15/99 #2 LOW FLOW 6/15/99 REPLACED PUMP
6/15/99 #7 LOW FLOW 6/15/99 NO WATER
6/23/99 #9 NO FLOW 6/23/99 RESET CONTROLS
REPLACED PUMP ,METER &CLEANED
6/28/99 #3 LOW FLOW 6/28/99 LINES
6/28/99 #6 LOW FLOW 06/28/99 CLEANED LINES
6/28/99 #8 LOW FLOW 06/28/99 NEW PUMP
MECHANIC
L.B.
L.B.
L.B.
L.B.
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I Attachment 2
I Analytical Data for the
I January and April 1999 Sampllng Events
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,I Kubal-Furr & Associates
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DAYIS
FLOYD
Date:
Client:
LABORATORY ANALYSIS REPORT
Data Package
Groundwater and Sludge Analysis
February 11, 1999
HNA Holdings, Inc.
Shelby, North Carolina
D&F Project No.: 60885.00
000001
I Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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Df\YIS
FLOYD LABORATORY ANALYSIS REPORT
Contents
Groundwater (Level 2)
• Master Tracking List
• Sample Results
• Method Conformance Summary
• Batch Quality Control Data
Sludge (Level 3)
• Master Tracking List
• Sample Results
• Case Narrative
• Instrument QC Assessment Summary
• Batch Quality Control Data
Other Documentation
• Field Notes
• Chain-of-Custody(s)
000002
I Davis & Floyd, Inc. I PO Drawer 428 \ Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I {864) 229-441 3 I Fax [phone]
Df\YIS
FLOYD LABORATORY ANALYSIS REPORT
Groundwater (Reporting Level 2)
000003
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 \ 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone] I
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DAYIS
FLOYD
January 21, 1999
JERRY MCMURRAY
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
:L99011501
:60885.00
LABORATORY ANALYSIS REPORT
Login Number
Project Number
Description :GROUNDWATER SAMPLING & ANALYSIS
Dear Jerry Mcmurray:
We are pleased to provide the enclosed analytical results for the samples received by
Davis & Floyd, Inc. on January 15, 1999.
A formal Quality Assurance/Quality Control program is maintained by Davis & Floyd,
which is designed to meet or exceed the EPA or appropriate regulatory requirements.
All analytical analyses for this project met QA/QC criteria unless otherwise stated in the
footnotes. This report is to be reproduced only in full.
Feel free to contact our Client Services ReIJresentative at [phone] if further
explanation of the analysis is required. Unless other arrangements have been made, samples
wi1l be disposed of or returned f4 days from the date of the report. We appreciate the
opportunity to provide services to your firm.
Sincere!)',
DAVIS & F/4C
Cl~,,.if!/
Laboratory Manager
000001
I Davis & Floyd, Inc. ) PO Drawer 428 I Greenwood, SC 29648 ! 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229·4413 I Fax (864) 229•7119
Di\YlS
FLOYD LABORATORY ANALYSIS REPORT
Master Tracking List
Client
Contact
Sample ID
L990115O1-Ol
Volatile Organics
SWB46 8260B
L99O115O1-O2
Volatile Organics
SW846 8260B
L99011501-03
Volatile Organics
SW846 8260B
L99011501-04
Volatile Organics
SWB46 B260B
L99011501-05
Volatile Organics
SWB46 8260B
L99011501-06
Volatile Organics
SW846 8260B
Wet Chemistry
SW846 9060
L99011501-07
Volatile Organic•
SW846 8260B
HNA HOLDINGS INC,
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID
AA-54
CC-33
FF-34
FF-62
ao-n
K-28
P-58
NC Certification Number: 25
Project Number: 60885.00
Report Date
Page 1 of 2
Date Collected
14-JAN-99 15:01
01/15/99
14-JAN-99 18: 01
01/15/99
14-JAN-99 16:01
01/15/99
14-JAN-99 16:01
01/15/99
14-JAN-99 15:01
01/15/99
14-JAN-99 17: 01
: January 21, 1999
1135
15-JAN-99
11S5
15-JAN-99
1215
15-JAN-99
1234
15-JAN-99
1254
15-JAN-99
01/15/99 1314
01/18/99 1105
14-JAN-99 17:01 15-JAN-99
01/15/99 1333
OOOOO~i
Davis & Floyd, Inc. · I PO Drawer 428 ] Greenwood, SC 29648 ] 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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DAYIS
FLtfYD LABORATORY ANALYSIS REPORT
Master Tracking List
Client
Contact
Sample ID
L99011501-0B
Volatile Organic•
SW846 8260B
Wet Chelllistry
SW846 9060
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID
V-23
NC Certification Number: 25
Project Number: 60885.00
Report Date
Page 2 of 2
January 21, 1999
Data Collected
14-JAN-99 18:01 15-JAN-99
01/15/99 1354
01/18/99 1200
000006
Davis & Floyd, Inc. I PO Drawer 428 l Greenwood, SC 29648 l 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
D.AYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: AA-54
Matrix
Paramater
Volatile Organics
SW84.6 8:Z60B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENB
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BlITANONE
2-HEXANONS
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMBTHANE
BROMOFORM
BROMOMBTHANB
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROBTHANB
CHLOROFORM
CHLOROMBTHANB
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENB (TOTAL)
GW/ChemW
NC Certification Number: 25
Project Number: 60885.00
Report Date
Page l of 1
Sample ID
January 21, 1999
L99011501-0l
Date Collected: 14-JAN-99 15:48
Date Received: 15-JAN-99
Result RDL Onita Analyst Date
' 0.0050 0 .0050 mg/1 PAP 01/15/99
' 0.0050 0. 0050 mg/1 PAP 01/15/99
' 0. 0050-0.0050 mg/1 PAP 01/15/99
' 0 .0050 0.0050 mg/1 PAP 01/15/99
' 0 .0050 0.0050 mg/1 PAP 01/15/99
' 0 .0050 0.0050 mg/1 PAP 01/15/99
' 0.0050 0.0050 mg/1 PAP 01/15/99
' 0.010 0.010 mg/1 PAP 01/15/99
' 0. 010 0.010 mg/1 PAP 01/15/99
' 0.0050 0.0050 mg/1 PAP 01/15/99
' 0.010 0.010 mg/1 PAP 01/15/99
' 0.0050 0.0050 mg/1 PAP 01/15/99
' 0.0050 0.0050 mg/1' PAP 01/15/99
' 0.0050 0.0050 mg/1 PAP 01/15/99
' 0.010 0.010 mg/1 PAP 01/15/99
' 0.0050 0,0050 mg/1 PAP 01/15/99
' 0.0050 0.0050 mg/1 PAP 01/15/99
' 0.0050 0.0050 mg/1 PAP 01/15/99
' 0.010 0.010 mg/1 PAP '01/15/99
' 0.0050 0.0050 mg/1 PAP 01/15/99
' 0.010 0.010 mg/1 PAP 01/15/99
' 0.0050 0.0050 mg/1 PAP 01/15/99
' 0.0050 0.0050 mg/1 PAP 01/15/99
' 0.0050 0.0050 mg/1 PAP 01/15/99
' 0.0050 0,0050 mg/1 PAP 01/15/99
' 0.0050 0.0050 mg/1 PAP 01/15/99
' 0.0050 0.0050 mg/1 PAP 01/15/99
' 0.0050 0.0050 mg/1 PAP 01/15/99
' 0.0050 0.0050 mg/1 PAP 01/15/99
' o. 0050 0.0050 mg/1 PAP 01/15/99
' 0 .0050 0.0050 mg/1 PAP 01/15/99
' 0.0050 0.0050 mg/1 PAP 01/15/99
' 0.010 0.010 mg/1 PAP 01/15/99
' 0.010 0.010 mg/1 PAP 01/15/99
' 0.0050 0.0050 mg/1 PAP 01/15/99
000007
Time
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
1135
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone] I
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Di\YIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: CC-33
Matrix
Volatil• Organics
514846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROSTHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANB
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANB
CHLOROFORM
CHLOROMETHANB
CIS-1,2-DICHLOROETHENE
CIS-1,3-0ICHLOROPROPBNB
OIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TBTRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENB
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENB
VINYL ACETATE
VINYL CHLORIDE
XYLENE {TOTAL)
GW/ChemW
NC Certification Number: 25
Result
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0. 010
' 0.010
' 0.0050
' 0. 010
' 0.0050
' 0.0050
' 0.0050
' 0. 010
' 0.0050
' 0.0050
' 0.0050
' 0.010
' 0.0050
' 0. 010
' 0 .0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.010
' 0.010
' 0.0050
000003
Project Number: 60885.00
Report Date
Pagel of 1
Sample ID
January 21, 1999
L99011501-02
Date Collected: 14-JAN-99 18:52
Date Received: 15-JAN-99
Qual RDL Units Analyst Date
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
0. 0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0. 010 mg/1 PAP 01/15/99
0. 010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0. 010 mg/1 PAP· 01/15/99
0.0050 mg/1 PAP 01/1S/99
0. 010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
o.ooso mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
Time
1155
1155
1155
1155
1155
1155
1155
1155
1155
1155
ll55
1155
1155
1155
1155
1155
1155
1155
1155
1155
1155
1155
1155
1155
1155
1155
1155
1155
1155
1155
1155
1155
1155
1155
1155
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 l 816 E. Durst Avenue I Greenwood, SC 29649 1 [phone] I Fax [phone]
DAYIS
FLOYD. LABORATORY ANALYSIS REPORT
client
Contact
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
client ID: FF-34.
Matrix
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANB
1,1,2,2-TETRACHLOROETHANB
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANB
1,1-DICHLOROBTHENB
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BlITANONE
2-HEXANONE
4-MBTHYL-2-PBNTANONB
ACETONE
BENZENE
BROMODICHLOROMBTHANB
BROMOFORM
BROMOMBTHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBBNZBNE
CHLOROBTHANB
CHLOROFORM
CHLOROMBTHANB
CIS-1,2-DICHLOROBTiiENB
CIS-1,3-DICHLOROPROPENB
DIBROMOCHLOROMETHANE
BTHYLBENZBNE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROBTHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROSTHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
GW/ChemW
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
' ' .
'
'
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'
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'
'
'
'
'
'
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'
'
'
'
NC Certification Number: 25
Project Number: 60895.00
Report Date January 21, 1999
Page l of 1
Sample ID L99011501-03
Date Collected: 14-JAN-99 16:55
Date Received ' 15-JAN-99
R•ault Qual RDL Unit• Analyst Oat• Time
0.0050 0 .0050 mg/1 PAP 01/15/99 1215
0.0050 0 .0050 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.010 0 .010 mg/1 PAP 01/15/99 1215
0.010 0.010 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.010 0.010 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.010 0.010 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0. 010 0.010 mg/1 PAP· 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.010 0. 010 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.0050 0 . 0050 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.0050 0 .0050 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
0.0050 0.0050 mg/1 PAP 01/15/99 1215
·0.010 0.010 mg/1 PAP 01/15/99 1215
0.010 0.010 mg/1 PAP 01/15/99 1215
o.ooso 0.0050 mg/1 PAP 01/15/99 1215
ooooon
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Davis & Floyd, Inc. ! PO Drawer 428 l Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone] I
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DL\YIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
RNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: FF-62
Matrix
Parameter
Volatile Organic•
SW846 8260B
1,1,l·TRICHLOROBTHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROBTHANE
1,1-DICHLOROETHENB
'i, 2-DICHLOROETHANE
1,2-DICHLOROPROPANB
2-BlITANONB
2-HBXANONE
4-METHYL-2-PBNTANONE
ACETONE
BENZENE
8ROMOOICHLOROMETHANB
BROMOFORM
BROMOMBTHANB
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBBNZENE
CHLOROETHANE
CHLOROFORM
CHLOROMBTHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-0ICHLOROPROPBNB
DIBROMOCHLOROMBTHAflB
BTHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENB
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROBTHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
GW/ChemW
NC Certification Number: 25
Re•ult
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0. 010
' 0.010
' 0.0050
' 0.010
' 0.0050
' 0. 0050
' 0 .0050
' 0.010
' 0.0050
' 0.0050
' 0.0050
' 0. 010
' 0.0050
' 0.010
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.0050
' 0.010
' 0.010
' 0.0050
000010
Project Number: 60885.00
Report Date
Page 1 of 1
Sample ID
January 21, 1999
L99011501-04
Date Collected: 14-JAN-99 16:47
Date Received: 15-JAN-99
Qual RDL Onita .Analyst Date
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0. 010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0. 010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0. 010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
Time
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
1234
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue 1 Greenwood, SC 29649 I [phone] I Fax [phone]
I
Df\VIS
FLtrYD LABORATORY ANALYSIS REPORT I
Client
Contact
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: GG-61
Matrix
Volatil• Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETH.ANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETH.ANE
1,1-DICHLOROETHENE
1,2-DICHLOROSTHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONS
4-MBTHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETH.ANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMBTHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-0ICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3·DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
GW/ChemW
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648
<
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<
<
<
<
<
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<
<
<
<
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NC Certification Number: 25
Project Number: 60885.00
Report Date
Page 1 of 1
Sample ID
: January 21, 1999
L99011501-0S
Date Collected: 14-JAN-99 15:18
Date Received : 15-JAN-99
Result Qual RDL Onita Analyst Date
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.010 0. 010 mg/1 PAP 01/15/99
0.010 0 .010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/i PAP 01/15/99
0.010 0. 010 mgn PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0 . 0050 mg/1 PAP 01/15/99
0. 010 0. 010 mg/1 PAP 01/15/99
0 .0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0. 010 0.010 mg/1 PAP· 01/15/99
0,0050 0.0050 mg/1 PAP 01/15/99
0. 010 0. 010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0 . 0050 mg/1 PAP 01/15/99
0.0050 0. 0050 mg/1 PAP 01/15/99
0.0050 0 . 0050 mg/1 PAP 01/15/99
0.0050 0 .0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0. 010 0. 010 mg/1 PAP 01/15/99
0.010 0.010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
000011
Time
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
1254
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l 816 E. Durst Avenue I Greenwood, SC 29649 I {864) 229-4413 1 Fax [phone] I
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DL\VIS
FLtJYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINas INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
client ID: K-28
Matrix
Parameter
Volatile Organics
SWB46 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROBTHANE
1,1-DICHLOROBTHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BlJTANONB
2-HBXANONB
~-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMBTHANE
~ BROMOFORM
BROMOMBTHANB
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENB
CHLOROETHANB
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENB
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENB
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Wet Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
GW/ChemW
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NC Certification Number: 25
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.010
0.010
0.0050
0. 010
0.010
0.0050
0.0050
0.010
0.0050
0.0050
0.0050
0.010
0.0050
0.010
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.010
0.010
0.0050
Project Nutnber: 60B85.00
Report Date
Page 1 of l
Sample ID
January 21, 1999
L99011501-06
Date Collected: 14-JAN-99 17:55
Date Received: 15-JAN-99
RDL Onits Analyst Dat•
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
0 . 0050 mg/1 PAP 01/15/99
0. 010 mg/1 PAP 01/15/99
0. 010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0. 010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0. 0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/9~
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0 .010 mg/1 PAP 01/15/99
0 .010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
Tim•
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
1314
s., 1.0 mg/1 TRB 01/18/99 1105
000012 I Davis·& Floyd, Inc. I PO Drawer 428 l Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 J (864) 229-44,13 I Fax [phone]
D1\_YIS
FLOYD LABORATORY ANALYSIS REPORT
client
Contact
HNA HOLDINOS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: P-58
Matrix
Parameter
Volatile Organics
SW8<!16' 8260B
1,1,l·TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONB
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOOICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENS
CHLOROETHANB
CHLOROFORM
CHLOROMB'THANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANB
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1, 2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
GW/ChemW
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NC Certification Number: 25
Project Number: 60885.00
Report Date
Page 1 of 1
Sample ID
January 21, 1999
L99011501-07
Date Collected: 14-JAN-99 17:28
Date Received: 15-JAN-99
Re ■ult Qual RDL Unit• Analyst Date
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0. 010 0.010 mg/1 PAP 01/15/99
0. 010 0.010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.010 0.010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0. 010 0.010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.010 0.010 mg/1 PAP· 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.010 0.010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0 .0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.010 0.010 mg/1 PAP 01/15/99
0.010 0.010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
000013
Ti>n•
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
1333
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 [ 816 E. Dursl Avenue I Greenwood, SC 29649 I (864) 229•4413 I Fax (864) 229•7119 I
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D1\VIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 2B150
JERRY MCMURRAY
Client ID: V-23
Matrix
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANB
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
., 1,2-DICHLOROETHANE
.. 1,2-DICHLOROPROPANE
2-BUTANONB
2-HEXANONB
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANB
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENB
CHLOROETHAN'E
CHLOROFORM
CHLOROMETHAN"E
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
OIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Wet Ch.miatry
SW846 9060
ORGANIC CARBON, TOTAL
GW/ChemW
NC Certification Number: 25
0.010
0. 010
0.010
0.010
0.010
0. 010
0.010
0.34
0.020
0.010
0,020
0.014
o. 010
0,010
0.020
0. 010
0.010
0.010
0.020
0. 010
0.020
0.010
0. 010
0.010
0.010
0.010
0.010
0.010
0. 010
0.010
0.010
0.010
0,020
0.020
0. 010
5810
Project Number: 60885.00
Report Date
Page 1 of 1
Sample ID
: January 21, 1999
L99011501-08
Date Collected: 14-JAN-99 18:24
Date Received : 15-JAN-99
Qual
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
RDL
0.010
0. 010
0.010
0.010
0.010
0. 010
0.010
0.020
0.020
0.010
0.020
0.010
0.010
0. 010
0.020
0. 010
0.010
0.010
0.020
0. 010
0.020
0.010
0.010
o. 010
0.010
0. 010
0.010
0.010
0. 010
0.010
0.010
0.010
o. 020
0.020
0. 010
100
Unit ■ Analy■t Date Time
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
PAP Ol/iS/99 135-4
PAP 01/15/99 135-4
PAP 01/15/99 135-4
PAP 01/15/99 135-4
PAP 01/15/99 135-4
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 135-4
PAP 01/15/99 1354
PAP Ol/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP ·Ol/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 135-4
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
PAP 01/15/99 1354
TRB 01/18/99·1200
000011
·-I Davis & Floyd, lnc. I PO Drawer 428 [ Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 [ [phone] I Fax [phone]
Di\YIS
FLtn'D LABORATORY ANALYSIS REPORT
Method Conformance Summary
Client: HNA HOLDINGS, INC.
Login: L99011501
Semi
Critetria Volatiles Volatiles Metals
Sample Holding Time ✓ NIA NIA
Standards Preparation ✓ NIA NIA
Instrument Tuning ✓ NIA NIA
Instrument Calibration ✓ NIA NIA
Calibration Verification ✓ NIA NIA
Degradation Check NIA NIA NIA
Interference NIA NIA NIA
Sample/Standard
Blanks Results " NIA NIA
Method Accuracy " NIA NIA
Method Precision " NIA NIA
Surrogate Recovery ✓ NIA NIA
PDS/SD/MSA NIA NIA NIA
TCLP Preparation NIA NIA NIA
Key ✓ = Met Criteria Met
NI A = Not Applicable
• = Method Criteria Not Met -See footnote(s) below.
PDS = Post Digestion Spike
SD = Serial Dilution
MSA = Method of Standard Additions
Footnotes: TOC analyses are performed in the inorganics area.
000015
Project Number: 60885.00
Report Date: January 21, 1999
Inorganics Other
" NIA
" NIA
NIA NIA
" NIA
" NIA
NIA NIA
NIA NIA
✓ NIA
✓ NIA
✓ NIA
NIA NIA
NIA NIA
NIA NIA
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Davis & Floyd, Inc. I· PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone] I
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Df\VIS
FLOYD
Method Blanks
Blank
Para.meter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANB
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-0ICHLOROPROPANB
2-BtITAN0NE
2-HEXANONB
4-MBTHYL-2-PBNTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANB
BROMOFORM
BROMOMBTHANB
CARBON DISULFIDE
CARBON TBTRACHLORIDB
CHLOROBENZENE
CHLOROBTHANE
CHLOROFORM
CHLOROMBTHANE
CIS-1,2-DICHLOROETHBNE
CIS-1,3-DICHLOROPROPENB
OIBROMOCHLOROMETHANE
ETHYLBENZENB
METHYLENE CHLORIDE
STYRENE
TBTRACHLOROETHENE
TOLUENE
TRANS-1,2-0ICHLOROETHENB
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
MB1586B:1
LABORATORY ANALYSIS REPORT
Report Date ' January 21, 1999
Page 1 of 1
Matrix GW/ChemW
WorkGroup: WG15868
Cone Qual RDL Uni ta .Analyst Date Time
< 0.0050 0 .0050 mg/1 PAP 01/15/99 0934
< 0.0050 0. 0050 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.010 0.010 mg/1 PAP 01/15/99 0934
< 0. 010 0.010 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.010 0.010 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.010 0.010 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.0050 0. 00 50 mg/1 PAP 01/15/99 0934
< 0.010 0.010 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP ·01/15/99 0934
< 0. 010 0.010 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.0050 0 .0050 mg/1 PAP 01/15/99 0934
< 0.0050 0 .0050 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0 . 0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
< 0.010 0. 010 mg/1 PAP 01/15/99 0934
< 0. 010 0.010 mg/1 PAP 01/15/99 0934
< 0.0050 0.0050 mg/1 PAP 01/15/99 0934
00001G
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS
1,1-DICHLOROETHENE
BENZENE:
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
LCS15868:l
20.00
20.00
20.00
20.00
20.00
19. 65
19.77
19.36
19. 70
19.69
Report Date : January 21, 1999
Page 1 of l
Matrix GW/ChemW
WorkGroup: WG15B68
Method SW846 82608
98.3
98.9
96.8
98.5
98.5
000017
70-126
85-121
82-119
83-122
81-122
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I GreenwQ?d, SC 29649 I [phone] I Fax [phone] I
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
MS99011501-01:1586B
MSD99011501-0l:15868
so.oo
so.co
SO.OD
so.co
50. 00
50.00
SO.OD
SO.OD
SO.OD
so.co
Report Date
Page 1 of 1
: January 21, 1999
Matrix GW/ChemW
WorkGroup: WG15B68
Method SWS-46 8260B
< 0.00500 47.76
< 0.00500 47.23
< 0.00500 47.67
< 0.00500 49.21
< 0.00500 48.62
49. 33
50. 72
50 .11
51. 34
50.60
98.7
101. 4
100.2
102.7
101. 2
000018
95.S
94.5
95.3
98.4
97.2
3.23
7.13
4. 99
4.24
3.99
74-125
83-123
02-120
84-120
83-123
12
10
12
10
11
74-125
83-123
82-120
84-120
B3-123
Davis & Floyd, Inc. I PO Drawer 428 l Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 1 [phone] I Fax {864) 229-7119
Di\YIS
FLOYD LABORATORY ANALYSIS REPORT
Surrogates % Recovery
L99011501-0l 15-JAN-99 11: 35
L99011S01-02 15-JAN-99 11:SS
L99011501-03 15-JAN-99 12:15
L99D11501-04 15-JAN-99 12:34
L99011501-05 15-JAN-n 12: 54
L99011501·06 15-JAN-99 13 : 14
L99011501-07 15-JAN-99 13:33
L99011501-08 15-JAN-99 13:54
LCS15868:l 15-JAN-99 18:09
MB15868:l 15-JAN-99 09: 34
MS99011501-0l:15868 15-JAN-99 10: 56
MSD99011501-0l:15868 15-JAN-99 11:16
DCB 1,2-DICHLOROETHANE-D4
BFB BROMOFLUOROBENZENE
TOL TOLUENE-DB
90.5
98.8
97.1
99.2
100.1
101. 7
101. l
105. 4
105 .J
99.8
89.3
%.7
93.8
93.6
93.2
93 .8
94.0
93.9
94.6
99.7
92 .9
91.3
91.9
93.1
Report Date
Page 1 of 1
Matrix
Method
96. 7
97.S
96.6
97. 4
97. 7
96.1
95.6
93.7
93.7
94.l
95. 6
94,0
000019
; January 21, 1999
GW/ChemW
SW846 8260
Davis & Floyd, Inc. 1 PO Drawer 428 1 Greenwood, SC 29648 I 816 E. Durst Avenue f Greenwood, SC 29649 I [phone] I Fax [phone]
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FLffi7D
Method Blanks
Para.meter
Wet Chami•try
SW846 9060
Blank
ORGANIC CARBON, TOTAL
: MB15895:l
LABORATORY ANALYSIS REPORT
Cone
1.0
Report Date : January 21, 1999
Page 1 of 1
Matrix GW/ChemW
WorkGroup: WG15895
Qual RDL Units Analyst Date Time
1.0 mg/1 TRB 01/1B/99 1555
000020
Davis & Floyd, lnc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] l Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
LaboraJory Control Standards and DuplicaJes
LCS LCS15895:l
ORGANIC CARBON, TOTAL 10.00 10. 90
Report Date : January 21, 1999
Page 1 of 1
Matrix : GW/ChemW
WorkGroup: WG15895
Method : SW846 9060
109.0 90-110
000021
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648. I 816 E. Durst Avenue I Greenwood, SC 29649 I 1864) 229-4413 I Fax [phone] I
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FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSO
ORGANIC CARBON, TOTAL
ORGANIC CARBON, TOTAL
MS99011503-0l:15895
MSD99011503-0l:15B95
20.00
20.00
1. 95
20. 30
Report Date
Page 1 of 1
January 21, 1999
Matrix GW/ChemW
WorkGroup: WG15895
Method SW846 9060
21. 30 96. 8 74-132
91. 8 4.81 11 74-132
000022
I Davis & Floyrl, Inc. 1 PO Drawer 428 I Greenwood, SC 29648 1 816 E. Durst Avenue \ Greenvmod, SC 29649 ! [phone] I Fax [phone]
Di\VIS
FLtfi'D
February O 1, 1999
JERRY MCMURRAY
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
:L99011502
:60885.00
LABORATORY ANALYSIS REPORT
Login Number
Project Number
Description :GROUNDWATER/WASTEWATER SAMPLING & ANAL YSJS
Dear Jerry Mcmurray:
We are pleased to provide the enclosed analytical results for the samples received by
Davis & Floyd, Inc. on January 14, 1999.
A formal Quality Assurance/Quality Control program is maintained by Davis & Floyd,
which is designed to meet or exceed the EPA or appropriate regulatory requirements.
All ana!yticar analyses for this project met QA/QC criteria unless otherwise stated in the
footnotes. This report is to be reproduced only in full. .
Feel free to contact our Client Services Representative at [phone] if further
explanation of the analysis is required. Unless other arrangements have been made, samples
will be disposed of or returned f4 days from the date of the report. We appreciate the
opportunity to provide services to your firm.
Sincerely,
DA VIS & FLOYD 1NC.
if~
hn H. McCord, Jr.
boratory Manager
000023
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 [ (864) 229-441 3 I Fax [phone] I
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DAYIS
FLffi1D LABORATORY ANALYSIS REPORT
Master Tracking List
Client
Contact
Sample ID
L99011502-01
Volatile Organics
SWB46 8260B
Volatile Organics
SW846 8260B
Volatile Organics
SWB46 8260B
Volatile Organics
SW846 8260B
Volatile Organics
SW846 8260B
Wet Chemistry
SW846 9060
L99011502-06
Volatile Organics
SW846 8260B
Wat Chemistry
SW846 9060
L9901 -07
Pesticides and Herbicides
SWB46
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
client ID
HH-77
HH-77 D'CIP.
HH-48
ITCI
SBR SLUDGE
NC Certification Number: 25
Project Number: 60885.00
Report Date February 01, 1999
Page 1 of )
Date Collected Date Received
14-JAN-99 10:01 14-JAN-H
01/15/99 1413
14-JAN-99 10:01
01/15/99 1432
14-JAN-99 10:01 14-JAN-99
01/15/99 1452
01/15/99 1512
14-JAN-99 11:01 14-JAN-99
01/15/99 1532
01/18/99 1235
14-JAN-99 11: 01
01/20/99 1704
01/18/99 1343
14-JAN-99 11:01 14-JAN-H
000021
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29(,48 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
Df\VIS
FLOYD LABORATORY ANALYSIS REPORT
Master Tracking List
client
Contact
Sampl• ID
SW846 1311/8270C
Trace Metals TCLP
SW846 1311
L99011502-08
Semivolatile Organics
SW846 8270C
Volatile Organics
SW846 8260B
L99011502-09
Semivolatile Organics
SW846 8270C
Volatile Organics
SW846 8260B
L99011502-l0
Semivolatile Organics
SW846 8270C
Volatile Organics
SW846 8260B
L99011502-ll
S•mivol•tile Organics
SWB46 B270C
Volatile Organics
SW846 8260B
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID
PEW-1
PEW-4
PEW-4 DUP.
NC Certification Number: 25
Project Number: 60885.00
Report Date
Page 2 of 3
: February 01, 1999
Date Collected Da.te Received
~0;_1C,s,',if°Il211
19/99 1655
01/20/99 0947
14-JAN-99 11:01 14-JAN'-99
01/21/99 1306
01/15/99 1611
14-JAN-99 12:01 14-JAN-99
01/21/99 1346
01/15/99 1631
14-JAN-99 12:01 14-JAN-99
01/21/99 1425
01/15/99 1650
14-JAN-99 12:01 14-JAN-99
01/21/99 1504
01/15/99 l 710
000025
Davis & Floyd, Inc. ! PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 l [phone] I fax [phone]
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FLtJ\'D LABORATORY ANALYSIS REPORT
Master Tracking List
client
Contact
Sample ID
L99011502-12
Semivolatile Organics
SW846 B270C
Volatile Organics
SW846 8260B
L99011S -13
Pesticides
SWS46
SWB46 1311/BlSlA
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID
FP SLUDGE
TCLP
Semivolatila organics TCLP
SW846 1311/B270C
Volatile Organics
SWB46 8260B
L99011502-1S
Volatile Organics
SW846 8260B
L99011502-16
Volatile Organics
SW846 8260B
T-35
TRIP BLANK
NC Certification Number: 25
Project Number; 60885.00
Report Date
Page 3 of 3
February 01, 1999
Date Received
14-JAN-99 12:01 14-JAN-99
01/21/99 1543
01/15/99 1730
14-JAN-99 12:01 14-JAN-99
01/25/99 1401
01/19/99 1659
14-JAN-99 13:01
01/15/99 1750
14-JAN-99 14:01 14-JAN-99
01/19/99 1733
15-JAN-99
Dl/H/99 1714
00002G I Davis & Floyd, Inc. I PO D,awer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
Df\YIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: HH-77
Matrix
Parameter
Volatile Organics
SWB46 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROET!W-lE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENB
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONB
4-METHYL-2-PENTANONB
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANB
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENB
CHLOROBTHANB
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENB
CIS-1,3-DICHLOROPROPENB
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TBTRACHLOROETHENE
TOLUENE
TRANS-1,2·DICHLOROBTHBNE
TRANS-1,3-DICHLOROPROPENB
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
GW/ChemW
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
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<
<
<
<
<
<
<
<
<
<
<
<
NC Certification Number: 25
Project Number: 60865.00
Report Date
Page 1 of 1
Sample ID
: February 01, 1999
L990l15D2-0l
Date Collected: 14-JAN-99 10:42
Date Received: 14-JAN-99
Qual RDL Units 11.nalyat Date
0.0050 0 .0050 mg/1 PAP 01/15/99
0.0050 0 .0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0 .0050 mg/1 PAP 01/15/99
0.0050 0 .0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.010 0.010 mg/1 PAP 01/15/99
0. 010 0.010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0. 010 0. 010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.010 0. 010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.010 0. 010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.010 0.010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0 .0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0. 0050 mg/1 PAP 01/15/99
0.13 0.0050 mg/1 PAP 01/15/99
0.010 0.010 mg/1 PAP 01/15/99
0.010 0.010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
000027
Time
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
1413
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] J Fax [phone]
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FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
P.O. BOX B7
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: HH-77 PUP.
Matrix
Parameter
Volatile Organics
SW846 8260B
1,1,l·TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONB
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETH.ANE
crs-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENS
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENB
TOLUENE
TRANS-1,2-0ICHLOROBTHENB
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
GW/ChemW
<
<
<
<
<
<
<
<
<
<
<
<
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<
<
<
<
<
<
<
<
<
<
<
<
NC Certification Number: 25
Result
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.010
0 .010
0.0050
0.010
0.0050
0.0050
0.0050
0.010
0.0050
0.0050
0.0050
0.010
0.0050
0.010
0,0050
0.0050
0.0050
0.0050
0. 0050
o. 0050
0.0050
0.0050
0.0050
0.0050
0.13
0. 010
0.010
0.0050
Project Number: 60885.00
Report Date
Page 1 of 1
: February 01, 1999
Sample ID L99011502-02
Date Collected: 14-JAN-99 10:42
Date Received : 14-JAN-99
Qual RPL Units J.nalyat Data
0 .0050 mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
0. 0050 mg/1 PAP 01/15/99
0 ,0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
o. 010 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0. 010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0. 010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP , 01/15/99
0. 010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
o.ooso mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0. 010 mg/1 PAP 01/15/99
o. 010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
00002&
Time
1432
1432
1432
1432
1432
1432
1432
1432
1432
1432
1432
1432
1432
1432
1432
1432
1432
1432
1432
1432
1432
1432
1432
1-432
1432
1432
1432
1432
1432
1432
1432
1432
1432
1432
1432
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 l 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
Df\YIS
FLtrYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: HH-48
Matrix
Parameter
Volatile Organics
SWB46 8260B
1,1,1-TRICHLOROBTHANB
1,1,2,2-TETRACHLOROBTHANB
1,1,2-TRICHLOROETHANB
1,1-DICHLOROBTHANE
1,1-DICHLOROETHENB
1,2-DICHLOROETHANB
1,2-DICHLOROPROPANB
2-BlITANONB
2-HBXANONB
4-MBTHYL-2-PENTANONS
ACETONE
BENZENE
BROMODICHLOROMBTHANB
BROMOFORM
BROMOMBTHANB
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBBNZBNB
CHLOROIITHANB
CHLOROFORM
CHLOROMBTHANE
CIS-1,2-DICHLOROBTHBNB
CIS-1,3-DICHLOROPROPENB
DIBROMOCHLOROMETHANB
BTHYLBBNZBNB
MBTHYLENB CHLORIDE
STYRENE
TBTRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROBTHBNE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROBTHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
GW/ChemW
'
'
'
'
'
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f!C Certification Number: 25
Project Number: 608B5.00
Report Date
Page l of 1
Sample ID
: February 01, 1999
L99011502-03
Date Collected: 14-JAN-99 10:44
Date Received: 14-JAN-99
Result Qual RDL Unite .Analy11t Date
0.0050 0.0050 mg/1 PAP 01/15/99
0 .0050 0.0050 mg/1 PAP 01/15/99
0 .0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.010 0.010 mg/1 PAP 01/15/99
0.010 0.010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.010 0. 010 mg/1 PAP 01/15/99
0.0050 o.0050 mg/1 PAP 01/15/99
0.0050 0. 0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0. 010 0.010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.010 0.010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP· 01/15/99
0. 010 0. 010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0 .0050 0.0050 mg/1 PAP 01/15/99
0 .0050 0.0050 mg/1 PAP 01/15/99
0 .0050 0.0050 mg/1 PAP 01/15/9~
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
0.088 0.0050 mg/1 PAP 01/15/99
0. 010 0.010 mg/1 PAP 01/15/99
0.010 0.010 mg/1 PAP 01/15/99
0.0050 0.0050 mg/1 PAP 01/15/99
00002~)
Time
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
1452
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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D1\VIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: C-49
Matrix
Par-.JDeter
Volatile Organics
SWB46 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
l·, 2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMSTHANE
CIS-1,2-DICHLOROETHENS
CIS-1,3-DICHLOROPROPENS
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DlCHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
GW/ChemW
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NC Certification Number: 25
'
Result
0. 0050
0.0050
0 .00S0
0 . 0050
0.0050
0.0050
0.0050
0.010
0.010
o.ooso
0.010
o.ooso
D. 0050
0.0050
0.010
0.0050
0.0050
0.0050
0.010
0.0050
0.010
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.010
0.010
0.0050
Project Number: 60885.00
Report Date
Page 1 of 1
: February 01, 1999
Sample ID L99011502-04
Date Collected: 14-JAN-99 11:21
Date Received: 14-JAN-99
Qual RDL Units Analyst Date
0.0050 mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
0 .00S0 mg/1 PAP 01/15/99
o . 0050 mg/1 PAP 01/15/99
0 .ooso mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
0 .ooso mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0. 010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
o.ooso mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
o.ooso mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0.0050 mg/1 PAP ,01/15/99
0.010 mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
o.ooso mg/1 PAP 01/15/99
0 .ooso mg/1 PAP 01/15/99
0. 0050 mg/1 PAP 01/15/99
0 . 0050 mg/1 PAP 01/15/99
0. 0050 mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
0 .0050 mg/1 PAP 01/15/99
0.0050 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
0.010 mg/1 PAP 01/15/99
o.ooso mg/1 PAP 01/15/99
000030
Time
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
1512
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 [ [phone] / Fax [phone]
D1\VIS
FLtJYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC,
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITEF
Matrix : GW/ChemW
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOF'ORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROBTHANE
CHLOROFORM
CHLOROMBTHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROBTHENB
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
W•t Chemi•try
SW846 9060
ORGANIC CARBON, TOTAL
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
N,C Certification Number: 25
Result
0.0050
0.0050
0.0050
0 .00S0
0 .0050
0.0050
0.0050
0.010
0.010
0.00S0
0. 010
0.0050
0.0050
0.0050
0. 010
0.0050
0 . 0050
o. 0050
0.010
0.0050
0. 010
0.00S0
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.010
0.010
0.0050
Project Number: 60885.00
Report Date
Page 1 of 1
Sample ID
February 01, 1999
L99011502-0S
Date Collected: 14-JAN-99 11:38
Date Received: 14-JAN-99
Qual RDL Onita
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0 .00S0 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.010 mg/1 PAP
0. 010 mg/1 PAP
0.0050 mg/1 PAP
0.010 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0. 010 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.010 mg/1 PAP
0.0050 mg/1 PAP
0.010 mg/1 PAP
0 .0050 mg/1 PAP
o. 0050 mg/1 PAP
0.0050 mg/1 PAP
0 . 0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0 .0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0. 010 mg/1 PAP
0. 010 mg/1 PAP
0.0050 mg/1 PAP
Time
01/15/99 1532
01/15/99 1532
01/15/99 1S32
01/15/99 1532
01/15/99 1532
01/15/99 1532
01/15/99 1532
01/15/99 1S32
01/15/99 1532
01/15/99 1532
01/i5/99 1532
01/15/99 1532
01/15/99 1532
01/15/99 1532
01/15/99 1532
01/15/99 1532
01/15/99 1532
01/15/99 1532
01/15/99 1532
01/15/99 1S32
01/15/99 1S32
01/15/99 1532
01/15/99 1S32
01/15/99 1532
01/15/99 153 2
01/15/99 1S32
01/15/99 1532
01/15/99 1532
01/15/99 1532
01/15/99 1532
01/15/99 1532
Ol/1S/99 1532
01/15/99 1532
01/15/99 1532
01/15/99 153 2
1.0 mg/1 TRB 01/18/99 1235
000031
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Davis & Floyd, lnc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I 1864) 229-4413 I Fax [phone] I
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Df\VIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITCI
Matrix
Parameter
Volatile Organics
SW846 B260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANB
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2 -HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
.; BROMOMETHANB
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROBTHANB
CHLOROFORM
CHLOROMETHANB
CIS-1,2-DICHLOROBTHENB
CIS-1,J-OICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Wet Chemistry
SW84.6 9060
ORGANIC CARBON, TOTAL
GW/ChemW
<
<
<
<
<
<
<
<
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N,C Certification Number: 25
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0, 074
0.010
0.0050
0.010
0.035
0.0050
0.0050
0.010
0.0050
0 . 0050
0.033
0. 010
0.0050
0.010
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.010
0. 010
0.0050
Project Number: 60885.00
Report Date
Page 1 of 1
February 01, 1999
Sample ID L99011502-06
Date Collected: 14-JAN-99 11:41
Date Received: 14-JAN-99
Qual RDL Unita Analyst Date
o. 0050 mg/1 PAP 01/20/99
0 ,0050 mg/1 PAP 01/20/99
0.0050 mg/1 PAP 01/20/99
0.0050 mg/1 PAP 01/20/99
0.0050 mg/1 PAP 01/20/99
0.0050 mg/1 PAP 01/20/99
0.0050 mg/1 PAP 01/20/99
0.010 mg/1 PAP 01/20/99
0.010 mg/1 PAP 01/20/99
0.0050 mg/1 PAP 01/20/99
0.010 mg/1 PAP 01/20/99
0. 0050 mg/1 PAP 01/20/99
0 .0050 mg/1 PAP 01/20/':J9
0.0050 mg/1 PAP 01/20/99
0.010 mg/1 PAP 01/20/99
o. 0050 mg/1 PAP 01/20/99
o . 0050 mg/1 PAP 01/20/99
0 .0050 mg/1 PAP 01/20/99
0 .010 mg/1 PAP 01/20/99
0.0050 mg/1 PAP .01/20/99
0.010 mg/1 PAP 01/20/99
0.0050 mg/1 PAP 01/20/99
0.0050 mg/1 PAP 01/20/99
0.0050 mg/1 PAP 01/20/99
0.0050 mg/1 PAP 01/20/99
0.0050 mg/1 PAP 01/20/99
0.0050 mg/1 PAP 01/20/99
0.0050 mg/1 PAP 01/20/99
0 . 0050 mg/1 PAP 01/20/99
0.0050 mg/1 PAP 01/20/99
0.0050 mg/1 PAP 01/20/99
0.0050 mg/1 PAP 01/20/99
0.010 mg/1 PAP 01/20/99
o. 010 mg/1 PAP 01/20/99
0.0050 mg/1 PAP 01/20/99
Tim•
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1704
1620 100 mg/1 TRB 01/18/99 1343
00003~
Davis & Floyd, Inc. I PO Drawer 428 1 Greenwood, SC 29648 I 816 E. Durst Avenue \ Greenwood, SC 29649 I [phone] I Fax {864) 229-7119
D~S FL D LABORATORY ANALYSIS REPORT
I
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lf C Certification Number: 25 I
Client HNA HOLDINGS INC. Project Number: 60B85.00 I P.O. BOX 87
SHELBY, 'NC 281S0 Report Date February 01, 1999
Contact JERRY MCMURRAY Page 1 of 3 I client ID: PEW-1 Sample ID L99011502-08
Date Collected: 14-JAN-99 11: 57
Matrix GW/ChemW Date Received: 14-JAN-99 I
Parameter Result Qual RDL Onita Analyst Date Time
Semivolatile Organics I SW846 8270C
1, l' -BI PHENYL < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1306
1,2,4-TRICHLOROBENZENE < 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1306
1,2-DICHLOROBENZENE < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1306 I 1,3-DICHLOROBENZENE < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1306
1,4-DICHLOROBENZENE < 0.010 0 .010 mg/1 DSD/JRN 01/21/99 1306
2,4,S-TRICHLOROPHENOL < 0.010 0 .010 mg/1 DSD/JRN 01/21/99 1306 I 2,4,6-TRICHLOROPHENOL < 0.010 0.010 mg/1 DSO/JRN 01/21/99 1306
2,4-DICHLOROPHENOL < 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1306
2,4-DIMBTHYLPHENOL < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1306
2,4-DINITROPHENOL < 0.025 0.025 mg/1 DSD/JRN 01/21/99 1306 I 2,4-DINITROTOLUENE < 0 .010 . 0. 010 mg/1 DSD/JRN 01/21/99 1306
2,6-DINITROTOLUENE < 0 .010 0. 010 mg/1 DSD/JRN 01/21/99 1306
2-CHLORONAPHTHALENE < 0.010 0 .010 mg/1 DSD/JRN 01/21/99 1306
2-CHLOROPHBNOL < 0. 010 0.010 mg/1 DSD/JRN 01/21/99 1306 I 2-MSTHYL-4,6-DINITROPHBNOL < 0.025 0 .025 mg/1 DSD/JRN 01/21/99 1306
2-MBTHYLNAPHTHALENE < 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1306
2-METHYLPHENOL < 0.010 0. 010 mg/1 DSO/JRN 01/21/99 1306 I 2-NITROANILINE < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1306
2-NITROPHBNOL < 0.010 0.010 mg/1 oso/JRN 01/21/99 1306
3,3'-DICHLOROBENZIDINB < 0. 010 0.010 mg/1 DSD/JRN 01/21/99 1306
3-NITROANILINB < 0.010 0 .010 mg/1 DSD/JRN 01/21/99 1306 I 4-BROMOPHSNYL PHENYL BTHBR < 0.010 0 .010 mg/1 DSD/JRN 01/21/99 1306
4-CHLOR0-3-MBTHYLPHENOL < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1306
4-CHLOROANILINB < 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1306
4-CHLOROPHENYL PHENYL ETHER < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1306 I 4-METHYLPHBNOL < 0.010 0 .010 mg/1 DSD/JRN 01/21/99 1306
4-NITROANILINE < 0.010 0 .010 mg/1 DSD/JRN 01/21/99 1306
4-NITROPHENOL < 0.025 0.025 mg/1 OSD/JRN 01/21/99 1306
ACENAPHTHENB < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1306 I ACBNAPHTHYLENE < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1306
ANTHRACBNE < 0. 010 0. 010 mg/1 DSD/JRN 01/21/99 1306
BENZO{A)ANTHRACENB < 0. 010 0.010 mg/1 DSD/JRN 01/21/99 1306 I BBNZO(A)PYRBNB < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1306
BENZO(B)FLUORANTHENE < 0.010 0.010 mg/1 oso/JRN 01/21/99 1306
BENZO(G,H,I)PERYLENE < 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1306
BBNZO(K)FLUORANTHENB < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1306 I BENZOIC ACID < 0.050 0.050 mg/1 DSO/JRN 01/21/99 1306
BENZYL ALCOHOL < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1306
BIPHENYL ETHER < 0.010 o. 010 mg/1 DSD/JRN 01/21/99 1306
BIS(2-CHLOROETHOXY)MBTH.ANE < 0.010 0.010 mg/1 DSO/JRN 01/21/99 1306 I 000033
Davis & Floyd, lnc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I 18641 229-4413 I fax {8641 229--71191
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: PEW-1
Para.meter
BIS(2-CHLOROETHYL)ETHER
BIS(2-CHLOROISOPROPYL)ETHER
BIS(2-ETHYLHEXYL)PHTHALATE
BUTYL BENZYL PHTHALATE
CHRYSENE
DI-N-BUTYL PHTHALATE
DI-N-OCTYL PHTHALATE
DIBENZ{A,H)ANTHRACENE
DIBENZOFURAN
DIETHYL PHTHALATE
DIMETHYL PHTHALATE
FLUORANTHENE
FLUORENE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROCYCLOPENTADIENE
HEXACHLOROETHANE
INDENO(l,2,3-CD)PYRENE
ISOPHORONE
N-NITROSODI-N-PROPYLAMINE
N-NITROSODIPHENYLAMINE
NAPHTHALENE
NITROBENZENE
PENTACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRENE
Volatile Organiea
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
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N,C Certification Number: 25
Project Number: 60885.00
Report Date ' February 01, 1999
Page 2 of J
Sample ID L99011502-0B
Re•ult Qu•l RDL Units An•ly•t D•t• Tim•
0 .010 0.010 mg/1 DSD/JRN 01/21/99
0. 010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 o. 010 mg/1 DSD/JRN 01/21/99
0 .010 0.010 mg/1 DSD/JRN 01/21/99
.010 0.010 mg/1 DSD/JRN 01/21/99
0 .010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0, 010 mg/1 DSD/JRN 01/21/99
0 .010 0 .010 mg/1 DSD/JRN 01/21/99
0 .010 0, 010 mg/1 DSD/JRN 01/21/99
0. 010 0.010 mg/1 DSD/JRN 01/21/99
0 .010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0 .010 0 .010 mg/1 DSD/JRN 01/21/99
0. 010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0 .010 mg/1 DSD/JRN 01/21/99
0. 010 0. 010 mg/1 DSD/JRN 01/21/99
0. 010 0.010 mg/1 DSO/JRN 01/21/99
0. 010 0.010 mg/1 DSD/JRN 01/21/9':J
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0 .010 0.010 mg/1 DSD/JRN 01/21/99
0 .025 O. 02 5 mg/1 DSO/JRN 01/21/99
0.010 0.010 mg/1 oso/JRN 01/21/99
o. 010 0.010 mg/1 DSD/JRN 01/21/99
0 .010 0.010 mg/1 OSD/JRN 01/21/99
0.0050 0.0050 mg/1 PAP 01/15/9':J 1611
0.0050 0.0050 mg/1 PAP 01/15/99 1611
0.0050 0.0050 mg/1 PAP 01/15/'IJ9 1611
0 .0050 0 . 0050 mg/1 PAP 01/15/99 1611
0 . 0050 0 . 0050 mg/1 PAP 01/15/99 1611
0 .0050 0 .0050 mg/1 PAP 01/15/99 1611
0. 0050 0.0050 mg/1 PAP 01/15/99 1611
0.010 0.010 mg/1 PAP 01/15/99 1611
0. 010 0.010 mg/1 PAP 01/15/'IJ9 1611
0.0050 o.ooso mg/1 PAP 01/15/99 1611
0.010 0. 010 mg/1 PAP 01/15/9':J 1611
0.0050 0.0050 mg/1 PAP 01/15/99 1611
000031
1306
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1306
1306
1306
1306
1306
1306
1306
1306
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1306
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1306
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1306
1306
1306
1306
Davis & Floyd, Inc. I PO Dcawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
D~S
I
FL D LABORATORY ANALYSIS REPORT I
NC Certification Number: 25
' I
Client HNA HOLDINGS INC. Project Number: 60885.00 I P.O. BOX 87
SHELBY, NC 28150 Report Date ' February 01, 1999
Contact JERRY MCMURRAY Page 3 of 3 I Client ID; PEW-1 Sample ID L99011502-0B
Parameter Result Qual RDL Units Analyst Date Time I BROMODICHLOROMETHANE < 0.0050 0.0050 mg/1 PAP 01/15/99 1611
BROMOFORM < 0.0050 0.0050 mg/1 PAP 01/15/99 1611
BROMOMETHANE < 0.010 0.010 mg/1 PAP 01/15/99 1611 I CARBON DISULFIDE < 0 .0050 0.0050 mg/1 PAP 01/15/99 1611
CARBON TETRACHLORIDE < 0 .0050 0.0050 mg/1 PAP 01/15/99 1611
CHLOROBENZENE < 0.0050 0.0050 mg/1 PAP 01/15/99 1611
CHLOROETHANE < 0.010 0.010 mg/1 PAP 01/15/99 1611 I CHLOROFORM < 0.0050 0.0050 mg/1 PAP 01/15/99 1611
CHLOROMETHANE < 0.010 0. 010 mg/1 PAP 01/15/99 1611
CIS-1,2-DICHLOROETHENE < 0 .0050 0.0050· mg/1 PAP 01/15/99 1611 I CIS-1,3-DICHLOROPROPENE < o. 0050 0 . 0050 mg/1 PAP 01/15/99 Hill
DI8ROMOCHLOROMETHANE < 0.0050 0 .0050 mg/1 PAP 01/15/99 1611
ETHYLBENZENE < 0.0050 0 .0050 mg/1 PAP 01/15/99 1611
METHYLENE CHLORIDE < 0.0050 0 .0050 mg/1 PAP 01/15/99 1611 I STYRENE < 0.0050 0 .0050 mg/1 PAP 01/15/99 1611
TETRACHLOROETHENE < 0.0050 0.0050 mg/1 PAP 01/15/99 1611
TOLUENE < 0.0050 0.0050 mg/1 PAP 01/15/99 1611
TRANS-1,2-DICHLOROETHENE ' 0 .0050 0 .0050 mg/1 PAP 01/15/99 1611 I TRANS-1,3-DICHLOROPROPENE < 0. 0050 0 .0050 mg/1 PAP 01/15/99 1611
TRICHLOROETHENE 0.0074 0 .0050 mg/1 PAP 01/15/99 1611
VINYL ACETATE < 0.010 0. 010 mg/1 PAP 01/15/99 1611
VINYL CHLORIDE < 0.010 0. 010 mg/1 PAP 01/15/99 1611 I XYLENE {TOTAL) ' 0.0050 0.0050 mg/1 PAP 01/15/99 1611
Prep Procedure Method Analyst Prep Date I
Analytical Prep Procedures:
8NA SEMIVOLATILES SWB-46 35008 JMT 01/19/99 1200 I DO\oITHERM SWB46 35008 JMT 01/19/99 1200
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I {864) 229-4413 I Fax [phone] I
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Di\YIS
FLtfYD LABORATORY ANALYSIS REPORT
Client
contact
HNA HOLDINGS INC,
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: F-55
Matrix GW/ChemW
Parameter
Semivolatil• Organics
SW846 B270C
1, 1' -BI PHENYL
1,2,4-TRICHLOROBENZENE
1, 2-DICHLOROBENZENB -:!·
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
1 2,4,6-TRICHLOROPHENOL
2,4-DICHLOROPHENOL
2,4-DIMETHYLPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-METHYL-4,6-DINITROPHENOL
2-METHYLNAPHTHALENE
2-METHYLPHENOL
2-NITROANILINE
2-NITROPHENOL
3,3'-DICHLOROBBNZIDINB
3-NITROANILINB
4-BROMOPHENYL PHENYL ETHER
4-CHLOR0-3-METHYLPHENOL
4-CHLOROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-MSTHYLPHENOL
4-NITROANILINE
4-NITROPHENOL
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
BENZO(A)ANTHRACENE
BENZO(A)PYRENE
BENZO(B)FLUORANTHENE
BENZO(G,H,I)PERYLENE
BENZO(K)FLUORANTHENE
BENZOIC ACID
BENZYL ALCOHOL
BIPHENYL ETHER
BIS(2-CHLOROETHOXY)METHANE
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NC Certification Number: 25
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Re•ult
10.8
0.010
0.010
0.010
0. 010
0.010
0. 010
0.010
0.010
0.025
0.010
0.010
0,010
0. 010
0.025
0 ,71
0. 010
0.010
0.010
0. 010
0.010
0.010
0.010
0. 010
0. 010
0.18
0.010
0 .025
0. 010
0. 010
0. 010
0.010
0. 010
0.010
0. 010
0.010
0.050
0.010
23.1
0.010
Project Number: 60885.00
Report Date
Page 1 of 3
Sample 10
: February 01, 1999
L99011502-09
Date Collected: 14-JAN-99 12:03
Date Received: 14-JAN-99
Qual RDL Analy•t Date Time
2.0 mg/1 DSD 01/22/99 1949
0.010 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
0. 010 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
0.025 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
0 .010 mg/1 DSD/JRN 01/21/99
0 . 025 mg/1 DSD/JRN 01/21/99
0.10 mg/1 DSD 01/22/99 2026
0.010 mg/1 DSD/JRN 01/21/99
0. 010 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
0. 010 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
0.10 mg/1 DSO 01/22/99 2026
0. 010 mg/1 DSD/JRN 01/21/99
0.025 mg/1 DSD/JRN 01/21/99
0 .010 mg/1 DSD/JRN 01/21/99
0. 010 mg/1 DSD/JRN 01/21/99
0. 010 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
0 .010 mg/1 DSD/JRN 01/21/99
0. 010 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
0.050 mg/1 DSD/JRN 01/21/99
0.010 mg/1 DSD/JRN 01/21/99
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
1346
2.0 mg/1 DSO 01/22/99 1949
0.010 mg/1 OSD/JRN 01/21/99 1346
00003G
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax {864) 229-7119
D1\YIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: F-55
Para.tneter
BIS{2-CHLOROETHYL)ETHER
BIS(2-CHLOROISOPROPYL)ETHER
BIS(2-ETHYLHEXYL)PHTHALATE
BUTYL BENZYL PHTHALATE
CHRYSENB
DI-N-BUTYL PHTHALATE
DI-N-OCTYL PHTHALATE
DIBENZ(A,H)ANTHRACENE
DIBENZOFURAN
DIETHYL PHTHALATE
DIMETHYL PHTHALATE
FLUORANTHENE
FLUORENE
HEX.ACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROCYCLOPENTADIENE
HBXACHLOROETHANE
INDENO(l,2,3-CO)PYRENE
ISOPHORONE
N-NITROSODI-N-PROPYLAMINB
N-NITROSODIPHENYLAMINE
NAPHTHALENE
NITROBENZENE
PENTACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRBNE
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
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NC Certification Number: 25
'
Project Number: 60885.00
Report Date February 01, 1999
Page 2 of 3
Sample ID L99011502-09
Result Qu.-1 RDL Unite Ana.lyet Date Time
0. 010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/I DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/I DSD/JRN 01/21/99
0.010 0.010 mg/1 • DSD/JRN 01/21/99
0.010 0 .010 mg/1 DSD/JRN 01/21/99
0.078 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0 .010 0.010 mg/1 DSD/JRN 01/21/99
o. 010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0 .010 0 . 010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0 .010 mg/1 DSD/JRN 01/21/99
0. 010 0 . 010 mg/1 DSD/JRN 01/21/99
0.010 o. 010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.34 0.10 mg/1 DSD 01/22/99 2026
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.025 0. 025 mg/1 DSD/JRN 01/21/99
0.010 o. 010 mg/1 DSD/JRN 01/21/99
0 .049 0.010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0.0050 0.0050 mg/1 PAP 01/15/99 Hi31
0. 0050 0.0050 mg/1 PAP 01/15/99 1631
0.0050 0.0050 mg/1 PAP 01/15/99 1631
0.0050 0.0050 mg/1 PAP 01/15/99 1631
0.0050 0.0050 mg/1 PAP 01/15/!:19 1631
0.0050 0.0050 mg/1 PAP 01/15/99 1631
0.0050 0.0050 mg/1 PAP 01/15/99 1631
0.010 0.010 mg/1 PAP 01/15/99 1631
0. 010 0.010 mg/1 PAP 01/15/99 1631
0.0050 0.0050 mg/1 PAP 01/15/99 1631
0.064 0.010 mg/1 PAP 01/15/99 1631
0.061 0.0050 mg/1 PAP 01/15/99 1631
000037
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1346
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1346 I
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue j Greenwood, SC 29649 I [phone] I Fax [phone] I
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Di\VIS
FLOYD
Client
Contact
Client ID:
Parameter
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
crs-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-0ICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL}
Prep Procedure
Analytical Prep Procedures:
BNA SEMIVOLATILES
DOWTHERM
LABORATORY ANALYSIS REPORT
l'{C Certification Number: 25
HNA HOLDINGS INC. Project Number: 60885.00
P.O. BOX 87
SHELBY, NC 28150 Report Date February 01, 1999
JERRY MCMURRAY Page 3 of 3
F-55 Sample ID L99011502-09
Reault Qual RDL Onita Malyat Date Time
< 0.0050 0 .0050 mg/1 PAP 01/15/99 1631
< 0.0050 0. 0050 mg/1 PAP 01/15/99 1631
0.010 0.010 mg/1 PAP 01/15/99 1631
< 0.0050 0 .0050 mg/1 PAP 01/15/99 1631
< 0 . 0050 0 . 0050 mg/1 PAP 01/15/99 1631
< o. 0050 0.0050 mg/1 PAP 01/15/99 1631
< 0.010 0.010 mg/1 PAP 01/15/99 1631
< 0.0050 o.ooso mg/1 PAP 01/15/!:19 1631
< 0.010 0.010 mg/1 PAP 01/15/99 1631
< 0.0050 0.0050 mg/1 PAP 01/15/99 1631
< 0.0050 0.0050 mg/1 PAP 01/15/'H 1631
< 0.0050 0.0050 mg/1 PAP 01/15/99 1631
< 0.0050 0,0050 mg/1 PAP 01/15/99 1631
0.0050 0.0050 mg/1 PAP 01/15/99 1631
0.0050 0.0050 mg/1 PAP 01/15/99 1631
< 0.0050 0.0050 mg/1 PAP 01/15/99 1631
< 0.0050 0.0050 rng/1 PAP 01/15/99 1631
< 0.0050 0.0050 mg/1 PAP 01/15/99 1631
0.0050 0.0050 mg/1 PAP 01/15/99 1631
< 0.0050 0.0050 mg/1 PAP 01/15/99 1631
< 0.010 0.010 mg/1 PAP 01/15/99 1631
< 0. 010 0.010 mg/1 PAP 01/15/99 1631
< 0.0050 0.0050 mg/1 PAP 01/15/99 1631
M•thod Analyst Prep Date
SW846 3500B JMT 01/19/99 1200
SW846 3500B JMT 01/19/99 1200
000038
Davis & Floyd, Inc. I PO Drawer 428 j Greenwood, SC 2964B I Bl 6 E. Durst Avenue I Greenwood, SC 29649 I (B64) 229-4413 I Fax (B64) 229-7119
Di\YIS
FLtJ\'D LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC,
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: PEW-4
Matrix
P•ra.meter
Semivolatile Organics
SW846 82?0C
GW/ChemW'
1, 1' ·BIPHENYL
1,2,4-TRICHLOROBENZENE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DICHLOROPHENOL
2,4-DIMETHYLPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-METHYL-4,6-DINITROPHENOL
2-METHYLNAPHTHALENE
2-METHYLPHENOL
2-NITROANILINE
2-NITROPHENOL
3,3'-DICHLOROBBNZIDINE
3-NITROANILINE
4-BROMOPHENYL PHENYL ETHER
4-CHLOR0-3-METHYLPHENOL
4-CHLOROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-METHYLPHENOL
4-NITROANILINE
4-NITROPHENOL
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
BENZO(A)ANTHRACENE
BENZO(A)PYRENE
BENZO(B)FLUORANTHENE
BENZO(G,H,I)PERYLENE
BENZO(K)FLUORANTHENE
BENZOIC ACID
BENZYL ALCOHOL
BIPHENYL ETHER
BIS(2-CHLOROETHOXY)METHANB
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N,C Certification Number: 25
Project Number: 60885.00
Repcrt Date
Page 1 of 3
Sample ID
February 01, 1999
L99011502-10
Date Collected: 14-JAN-99 12:08
Date Received 14-JAN-99
Result Qual RDL units Analyat Date
0,012 0.010 mg/1 DSD/JRN 01/21/99
0. 010 0.010 mg/1 DSD/JRN 01/21/99
0 .010 0 .010 mg/1 DSD/JRN 01/21/99
0. 010 0.010 mg/1 DSD/JRN 01/21/99
0 .010 0.010 mg/1 DSD/JRN 01/21/99
0 .010 0.010 mg/1 DSD/JRN 01/21/99
0. 010 0.010 mg/1 DSD/JRN 01/21/99
o. 010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0 . 025 0.025 mg/1 DSD/JRN 01/21/99
0. 010 0.010 mg/1 DSD/JRN 01/2~/99
0 .010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0. 010 0.010 mg/1 DSD/JRN 01/21/99
0.025 0.025 mg/1 DSD/JRN 01/21/99
0. 010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 OSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0 .010 0.010 mg/1 DSD/JRN 01/21/99
0 .010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0 . 010 0.010 mg/1 DSD/JRN 01/21/99
0. 010 o. 010 mg/1 DSD/JRN 01/21/S9
0 .010 0.010 mg/1 DSD/JRN 01/21/99
0. 010 o. 010 mg/1 DSD/JRN 01/21/99
0.025 0.025 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/s9
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0. 010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSO/JRN 01/21/99
0.010 0. 010 mg/1 OSD/JRN 01/21/99
o.oso 0 .050 mg/1 DSO/JRN 01/21/99
0. 010 0. 010 mg/1 DSD/JRN 01/21/99
0.039 0.010 mg/1 DSO/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
000039
1425
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone] I
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: PEW-4
Para.mater
BIS(2-CHLOROETHYL)ETHER
BIS(2-CHLOROISOPROPYL)ETHER
B15(2-ETHYLHEXYL)PHTHALATE
BlITYL BENZYL PHTHALATE
CHRYSENE
DI-N-BUTYL PHTHALATE
DI-N-OCTYL PHTHALATE
DIBENZ(A,H)ANTHRACENE
DIBENZOFURAN
DIETHYL PHTHALATE
DIMETHYL PHTHALATE
FLUORANTHENE
FLUORENB
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROCYCLOPENTADIENE
HEXACHLOROETHANE
INDENO(l,2,3-CD)PYRENE
ISOPHORONE
N-NITROSODI·N-PROPYLAMINE
N-NITROSODIPHENYL.AMINE
NAPHTHALENE
NITROBENZENE
PENTACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRENE
Volatila Organics
SWB-46 B260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-0ICHLOROETHANE
1,1-DICHLOROETHENE
1,2-0ICHLOROETHANE
1,2-0ICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
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l'{C Certification Number: 25
Project Number: 608B5.00
Report Date ' February O 1, 1999
Page 2 of 3
Sample ID L99011502-10
Re111ult Qual RDL tfnit111 Analy•t Date Time
0.010 0.010 mg/1 oso/JRN 01/21/99
0.010 0.010 mg/1 OSD/JRN 01/21/99
0.010 0.010 mg/1 oso/JRN 01/21/99
0. 010 0. 010 mg/1 DSO/JRN 01/21/99
0.010 0.010 mg/1 oso/JRN 01/21/99
0. 010 0.010 mg/1 oso/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0. 010 0 . 010 mg/1 OSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0. 010 0. 010 mg/1 OSD/JRN 01/21/99
0 . 010 0 . 010 mg/1 DSD/JRN 01/21/99
0.010 0 . 010 mg/1 DSD/JRN 01/21/99
0.010 0 .010 mg/1 DSD/JRN Ol/21/99
0. 010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSO/JRN 01/21/99
0.010 0. 010 mg/1 oso/JRN 01/21/99
0.010 0.010 mg/1 DSO/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 oso/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.025 0.025 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 o. 010 mg/1 oso/JRN 01/21/99
0.010 0 .010 mg/1 DSO/JRN 01/21/99
0.0050 0 . 0050 mg/1 PAP 01/15/99 1650
0.0050 0.0050 mg/1 PAP 01/15/99 1650
0.0050 0.0050 mg/1 PAP 01/15/99 1650
0.0050 0.0050 mg/1 PAP 01/15/99 1650
0.0050 0.0050 mg/1 PAP 01/15/99 1650
0.0050 0.0050 mg/1 PAP 01/15/99 1650
0.0050 0.0050 mg/1 PAP 01/15/99 1650
0.010 0. 010 mg/1 PAP 01/15/99 1650
0. 010 0.010 mg/1 PAP Ol/15/99 1650
0.0050 0.0050 mg/1 PAP 01/15/99 1650
0.010 0.010 mg/1 PAP 01/15/99 1650
0.0050 0.0050 mg/1 PAP 01/15/99 1650
000010
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Davis & Floyd, Inc. I PO Drawer 428 1 Greenwood, SC 29648 1 816 E. Durst Avenue I Greenwood, SC 29649 1 [phone] I Fax [phone]
DAYIS
FLt1YD
Client
Cont.act
Client IO:
Parameter
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Prep Procedure
Analytical Prep Procedure•:
BNA SEMIVOLATILES
DOWI'HERM
I
LABORATORY ANALYSIS REPORT I
l'{C Certification Number: 25 I
HNA HOLDINGS INC. Project Number: 60885.00
P.O. BOX 87 I
SHELBY, NC 28150 Report Date ' February 01, 1999
JERRY MCMURRAY Page 3 of 3
PEW-4 Sample ID L99011502-10 I
Reault Qual RDL Units Analyst Date Time
' 0.0050 o. 0050 mg/1 PAP 01/15/99 1650 I
' 0.0050 0 .0050 mg/1 PAP 01/15/99 1650
' 0.010 0. 010 mg/1 PAP 01/15/99 1650
' 0.0050 0.0050 mg/1 PAP 01/15/99 1650
' 0.0050 0.0050 mg/1 PAP 01/15/9!.I 1650 I
' 0.0050 0.0050 mg/1 PAP 01/15/<J9 1650
' 0.010 0. 010 mg/1 PAP 01/15/99 1650
' 0.0050 0.0050 mg/1 PAP 01/15/99 1650 I
' 0.010 0.010 mg/1 PAP 01/15/99 1650
0.011 0 .0050 mg/1 PAP 01/15/99 1650
' 0.0050 0 .0050 mg/1 PAP 01/15/99 1650
' 0.0050 0.0050 mg/1 PAP 01/15/99 1650 I
' 0.0050 0.0050 mg/1 PAP 01/15/99 1650
' 0.0050 0.0050 mg/1 PAP 01/15/99 1650
' 0.0050 0.0050 mg/1 PAP 01/15/99 1650
' 0.0050 0.0050 mg/1 PAP 01/15/99 1650 I
' 0.0050 0.0050 mg/1 PAP 01/15/99 1650
' 0.0050 0.0050 mg/1 PAP 01/15/99 1650
' 0.0050 0.0050 mg/1 PAP 01/15/99 1650 I
0 .091 0.0050 mg/1 PAP 01/15/99 1650
' 0.010 0. 010 mg/1 PAP 01/15/99 1650
' 0.010 0 .010 mg/1 PAP 01/15/99 1650
' 0.0050 0.0050 mg/1 PAP 01/15/99 1650
Method Analyst Prep Date I
SW846 3500B JMT 01/19/99 1200
SW846 3500B JMT 01/19/99 1200 I
I
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000041
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 ! 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
I
I DCMS
FL D LABORATORY ANALYSIS REPORT
I NC Certification Number: 25
'
I Client HNA HOLDINGS INC. Project Number: 60885.00
P.O. BOX 87
SHELBY, NC 28150 Repcrt Date February 01, 1999
I Contact JERRY MCMURRAY Page 1 of 3
Client ID: PEW-4 DUP. Sample ID L99011502-11
Date Collected: 14-JAN-99 12; 08
I Matrix GW/ChemW Date Received: 14-JAN-99
Parat11eter Result Qual RDL Unit• Analyst D•t• Time
I Seitlvolatile Organics
SWB46 8270C
1, l' -BI PHENYL < 0 .010 0.010 mg/1 DSD/JRN 01/21/99 1504
I 1,2,4-TRICHLOROBENZENE < 0.010 0. 010 mg/1 0S0/JRN 01/21/99 1504
1,2-DICHLOROBENZENE < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1504
1,3-DICHLOROBENZENE < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1504
1,4-DICHLOROBENZENE < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1504
I 2,4,5-TRICHLOROPHENOL < 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1504
2,4,6-TRICHLOROPHENOL < 0.010 o. 010 mg/1 DSD/JRN 01/21/99 1504
2,4-DICHLOROPHENOL < 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1504
2,4-DIMETHYLPHENOL < 0.010 0. 010 mg/1 DSO/JRN 01/21/99 1504
I 2,4-0INITROPHENOL < 0.025 o. 025 mg/1 DSD/JRN 01/21/99 1504
2,4-DINITROTOLUENE < 0.010 0 .010 mg/1 DSD/JRN 01/21/99 1504
2,6-DINITROTOLUENE < 0. 010 0.010 mg/1 DSO/JRN 01/21/99 1504
I 2-CHLORONAPHTHALENE < 0.010 0.010 mg/1 DSD/JRN Ol/2~/99 1504
2-CHLOROPHENOL < 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1504
2-METHYL-4,6-DINITROPHENOL < 0.025 0.025 mg/1 DSO/JRN 01/21/99 1504
2-MBTHYLNAPHTHALENE < 0,010 0.010 rng/1 DSD/JRN 01/21/99 1504
I 2-METHYLPHENOL < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1504
2-NITROANILINE < 0,010 0.010 mg/1 DSD/JRN 01/21/99 1504
2 -NITRO PHENOL < 0. 010 0.010 mg/1 DSD/JRN 01/21/99 1504
3,3'-DICHLOROBENZIDINB < 0.010 0 .010 mg/1 DSD/JRN 01/21/99 1504
I 3-NITROANILINE < 0. 010 o. 010 mg/1 DSD/JRN 01/21/99 1504
4-BROMOPHENYL PHENYL ETHER < 0. 010 0.010 mg/1 DSD/JRN Ol/21/'J9 1504
4-CHLOR0-3-METHYLPHENOL < 0. 010 0.010 mg/1 DSD/JRN 01/21/9'J 1504
I 4-CHLOROANILINE < 0.010 0 . 010 mg/1 DSD/JRN 01/21/99 1504
4-CHLOROPHENYL PHENYL ETHER < 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1504
4-METHYLPHENOL < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1504
4-NITROANILINE < 0. 010 0.010 mg/1 DSD/JRN 01/21/99 1504
I 4-NITROPHENOL < 0.025 0.025 mg/1 DSD/JRN 01/21/99 1504
ACENAPHTHBNB < 0.010 0.010 mg/1 DSD/JRN Ol/21/99 1504
ACENAPHTHYLBNE < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1504
ANTHRACENE < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1504
I BENZO(A)ANTHRACENE < 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1504
BENZO(A)PYRENE < 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1504
BENZO(B)FLUORANTHENE < 0.010 0.010 mg/1 DSD/JRN 01/21/99 1504
I BENZO(G,H,I)PERYLENB ' 0.010 0.010 mg/1 DSD/JRN Ol/21/99 1504
BENZO(K)FLUORANTHENE < 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1504
BENZOIC ACID < 0.050 0. 050 mg/1 DSD/JRN 01/21/99 1504
BBNZYL ALCOHOL < 0. 010 0. 010 mg/1 DSD/JRN 01/21/99 1504
I BIPHBNYL ETHER 0.034 0 .010 mg/1 DSD/JRN 01/21/99 1504
BIS(2-CHLOROETHOXY)METHANE < 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1504
000042
I Davis & Floyd, Inc. I PO Drawer 428 I G,eenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I 1864! 229.4413 I Fax [phone]
Df\YIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client IO: PEW-4 PUP.
Pilrailletor
BIS(2-CHLOROETHYL)ETHER
BIS(2-CHLOROISOFROPYL)ETHER
BIS{2-ETHYLHEXYL)PHTHALATE
BUTYL BENZYL PHTHALATE
CHRYSENE
DI-N-BUTYL PHTHALATE
DI-N-OCTYL PHTHALATE
DIBENZ(A,H)ANTHRACENE
DIBENZOFURAN
DIETHYL PHTHALATE
DIMETHYL PHTHALATE
FLUORANTHENE
FL~ORENE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROCYCLOPENTADIBNE
HEXACHLOROETHANE
INDENO(l,2,3-CD)PYRENE
ISOPHORONE
N-NITROSODI-N-PROPYLAMINE
N-NITROSODIPHENYLAMINE
NAPHTHALENE
NITROBENZENB
PENTACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRENE
Volatile Organic•
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-0ICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
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NC Certification Number: 25
'
Project Number: 60885.00
Report Date February 01, 1999
Page 2 of 3
Sample ID L99011502-11
R•ault Qual RDL Onita Analyat Dat• TUile
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0. 010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0. 010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0 .010 0.010 mg/1 DSD/JRN 01/21/99
0 .010 0.010 mg/1 DSD/JRN 01/21/99
0 .010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0.025 0. 025 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0. 0050 0.0050 mg/1 PAP 01/15/99 1710
0. 0050 0.0050 mg/1 PAP 01/15/99 1710
0.0050 0.0050 mg/1 PAP 01/15/99 1710
0.0050 0.0050 mg/1 PAP 01/15/99 1710
0.0050 0.0050 mg/1 PAP 01/15/99 1710
0 . 0050 0.0050 mg/1 PAP 01/15/99 1710
0.0050 0.0050 mg/1 PAP 01/15/99 1710
0. 010 0 . 010 mg/1 PAP 01/15/99 1710
0.010 o. 010 mg/1 PAP 01/15/99 1710
o.ooso 0.0050 mg/1 PAP 01/15/99 1710
0.010 0.010 mg/1 PAP 01/15/99 1710
0.0050 0.0050 mg/1 PAP 01/15/99 1710
000043
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1504 I
1S04
1504
1504
1504 I
1504
1504
1504 I
1504
1S04
1504
1504 I
1504
1504
1504
1504 I
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1504
1504 I
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1504
1504
1504 I
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1504
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1504 I
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Davis & Floyd, Inc. l PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I fax [phone]
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Df\YIS
FLtwD
Client
Contact
client ID:
Parameter
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
Prep Procedure
An•lytical Prep Procedures:
BNA SEMIVOLATILES
DOWI'HERM
LABORATORY ANALYSIS REPORT
N,C Certification Number: 25
HNA HOLDINGS INC. Project Number: 60885.00
P.O. BOX 87
SHELBY, NC 28150 Report Date February 01, 1999
JERRY MCMURRAY Page 3 of 3
PEW-4 DOP. Sample ID L99011502-ll
Result Qual RDL Onita Analyst Date Time
' 0.0050 0.0050 mg/1 PAP 01/15/'H 1710
' 0.0050 0.0050 mg/1 PAP 01/15/99 1710
' 0.010 0.010 mg/1 PAP Ol/1S/99 1710
' 0.0050 o. 0050 mg/1 PAP 01/15/99 1710
' 0.0050 0 .0050 mg/1 PAP 01/15/99 1710
' 0.0050 0 .0050 mg/1 PAP 01/15/99 1710
' 0.010 0.010 mg/1 PAP 01/15/99 1710
' 0.0050 0.0050 mg/1 PAP D1/15/99 1710
' 0. 010 0.010 mg/1 PAP 01/15/99 1710
0.011 0.0050 mg/1 PAP 01/15/99 1710
' 0.0050 0.0050 mg/1 PAP 01/15/99 1710
' 0.0050 0.0050 mg/1 PAP 01/15/99 1710
' 0.0050 0. 0050 mg/1 PAP 01/15/99 1710
' 0.0050 0 .0050 mg/1 PAP 01/15/99_ 1710
' 0.0050 0.0050 mg/1 PAP 01/15/99 1710
' 0.0050 0.0050 mg/1 PAP 01/15/99 1710
' 0.0050 0.0050 mg/1 PAP 01/15/99 1710
' 0.0050 0.0050 mg/1 PAP 01/15/99 1710
' 0.0050 0.0050 mg/1 PAP 01/15/99 1710
0.093 0.0050 mg/1 PAP 01/15/99 1710
' 0 .010 0 .010 mg/1 PAP 01/15/99 1710
' o. 010 0.010 mg/1 PAP 01/15/99 1710
' 0.0050 0.0050 mg/1 PAP 01/15/99 1710
Method An•lyat Prep Dato
SW846 35008 JMT 01/19/99 1200
SWB46 35008 JMT 01/19/99 1200
Davis & Floyd, Inc. I PO Drawer 428 l Greenwood, SC 29648 I 816 E. Durst Avenue l Greenwood, SC 29649 I [phone] I Fax [phone]
Di\VIS
FLi1YD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: PEW-3
Matrix
Parameter
Somivolatile Organics
SW846 8270C
: GW/ChemW'
1, 1' -BI PHENYL
1,2,4-TRICHLOROBENZENE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DICHLOROPHENOL
2,4-DIMETHYLPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-METHYL-4,6-DINITROPHENOL
2-METHYLNAPHTHALENE
2-MBTHYLPHENOL
2-NITROANILINE
2-NITROPHENOL
3,3'-DICHLOROBENZIDINB
3-NITROANILINB
4-BROMOPHENYL PHENYL ETHER
4-CHLOR0-3-MBTHYLPHENOL
4-CHLOROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-MBTHYLPHENOL
4-NITROANlLINE
4-NITROPHBNOL
ACENAPHTHENE
ACBNAPHTHYLENE
ANTHRACENE
BENZO(A)ANTHRACENE
BENZO(A)PYRENB
BBNZO(B)FLUORANTHENE
BENZO(G,H,I)PERYLENE
BBNZO(K)FLUORANTHENB
BENZOIC ACID
BENZYL ALCOHOL
BIPHENYL ETHER
BIS(2-CHLOROETHOXY)METHANE
l'{C Certification Number: 25
Project Number: 60885.00
Report Date February 01, 1999
Page 1 of 3
Sample ID L99011502-12
Date Collected: 14-JAN-99 12: 15
Date Received ' 14-JAN-99
Result Qual RDL Units Analyst Date Tim•
0. 010 o. 010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0. 010 0 .010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 .010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
o. 010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 osb/JRN 01/21/99
0.025 0 . 025 mg/1 DSD/JRN 01/21/99
0. 010 0 .010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN Ol./21/99
0. 010 0. 010 mg/1 DSD/JRN 01/21/99
0.025 0. 025 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0. 010 0.010 mg/1 DSD/JRN 01/21/99
0. 010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 O. Ol.O mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0. 010 0.010 mg/1 DSD/JRN 01/21/99
0. 010 0. 010 mg/1 oSD/JRN 01/21/99
0 .010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0. 010 0. 010 mg/1 DSD/JRN 01/21/99
0. 010 0.010 mg/1 DSD/JRN 01/21/99
0.025 0 .025 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0. 010 o. 010 mg/1 DSD/JRN 01/21/99
0. 010 0.010 mg/1 DSD/JRN 01/21/99
0. 010 0.010 mg/1 DSD/JRN 01/21/99
0,010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.050 0.050 mg/1 DSO/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
000045
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1543 I
1543
1543
1543 I
1543
1543
1543
1543 I
1543
1543
1543
l.543 I
1543
1543
1543 I 1543
1543
1543
l.543 I
1543
l.543
1543
1543 I
1543
1543
1543 I 1543
1543
1543
1543 I
1543
1543
1543
1543 I
1543
1543
1543
1543 I
1543
1543 I
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I 1864) 229-4413 I fax [phone]
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
RNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 2B150
JERRY MCMURRAY
Client ID: PEW-3
Pa:c:ani.eter
BIS(2-CHLOROETHYL}ETHBR
BIS(2·CHLOR0ISOPROPYL)BTHER
B1S(2-ETHYLHEXYL)PHTHALATE
BUTYL BENZYL PHTHALATE
CHRYSENE
DI-N-BlITYL PHTHALATE
DI-N-OCTYL PHTHALATB
DIBENZ(A,H)ANTHRACENE
DIBENZOFURAN
DIETHYL PHTHALATE
DIMETHYL PHTHALATE
FLUORANTHENE
FLUORENE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENB
HEXACHLOROCYCLOPENTADIENE
HEXACHLOROETHANE
INDENO(l,2,3-CO)PYRENE
ISOPHORONB
N·NITROSODI-N-PROPYLAMINE
N-NITROSODIPHENYLAMINB
NAPHTHALENE
NITROBENZENB
PENTACHLOROPHENOL
PHENANTHRENB
PHENOL
PYRENB
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANB
1,1,2,2-TETRACHLOROETHANB
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2·PENTANONE
ACETONE
BENZENE
<
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<
<
<
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<
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<
<
<
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<
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<
<
<
<
<
<
<
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!yC Certification Number: 25
Project Number: 60B85.00
Report Date February 01, 1999
Page 2 of 3
Sample ID L99011502-12
Result Oual RDL units An•lyst D•te Time
0.010 0 .010 mg/1 D50/JRN 01/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0. 010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0. 010 0.010 mg/1 D5D/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 D5D/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0. 010 0 .010 mg/1 DSD/JRN 01/21/99
0.010 0 .010 mg/1 DSD/JRN 01/21/99
0.010 0 .010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0 .010 0 .010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0 .010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN Ol/21/99
0.010 0. 010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0. 010 mg/1 OSD/JRN 01/21/99
0.010 0.010 mg/1 DSO/JRN 01/21/99
0.010 0 .010 mg/1 DSD/JRN 01/21/99
0.025 0. 025 mg/1 DSO/JRN 01/21/99
o. 010 0.010 mg/1 OSD/JRN 01/21/99
0.010 0.010 mg/1 DSD/JRN 01/21/99
0.010 0.010 mg/1 oso/JRN 01/21/99
0.0050 0.0050 mg/1 PAP 01/15/99 1730
0.0050 0.0050 mg/1 PAP 01/15/99 1730
0 .0050 0. 0050 mg/1 PAP 01/15/99 1730
0 . 0050 0 .0050 mg/1 PAP 01/15/99 1730
0.0050 0.0050 mg/1 PAP 01/15/99 1730
0.0050 0.0050 mg/1 PAP 01/1S/99 1730
0.0050 0.0050 mg/1 PAP 01/15/99 1730
0.010 0. 010 mg/1 PAP 01/15/99 1730
0. 010 0.010 mg/1 PAP Ol/1S/99 1730
0.0050 0.0050 mg/1 PAP 01/15/99 1730
0.010 0.010 mg/1 PAP 01/15/99 1730
0.0050 0.0050 mg/1 PAP 01/15/99 1730
00004G
1543
1543
1543
1543
1543
1543
1543
1543
1543
1543
1543
1543
1543
1543
1543
1543
1543
1543
1543
1543
1543
1543
1543
1543
1543
1543
1543
Davis & Floyd, lnc. 1 PO Drawer 428 1 Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
I
LABORATORY ANALYSIS REPORT I
NC Certification Number: 25
' I
client HNA HOLDINGS INC. Project Number: 60885.00
P.O. BOX 87
SHELBY, NC 28150 Report Date February 01, 1999 I
Contact JERRY MCMURRAY Page 3 of 3
client ID: PEW-3 Sample ID L99011502-12 I
Parameter Result Oual RDL Units Analyst Date Time
BROMODICHLOROMETHANE < 0 .0050 0.0050 mg/1 PAP 01/15/99 1730 I
BROMOFORM < 0. 0050 o.ooso mg/1 PAP 01/15/99 1730
BROMOMETHANE < 0.010 0.010 mg/1 PAP 01/15/99 1730
CARBON DISULFIDE < 0.0050 o.ooso mg/1 PAP 01/15/99 1730
CARBON TETRACHLORIDE < 0.0050 o.ooso mg/1 PAP 01/15/99 1730 I
CHLOROBSNZENE < o.ooso 0.0050 mg/1 PAP 01/15/99 1730
CHLOROETHANE < 0.010 0. 010 mg/1 PAP 01/15/99 1730
CHLOROFORM < Q.0050 0.0050 mg/1 PAP 01/15/99 1730 I
CHLOROMETHANE < 0.010 0.010 mg/1 PAP 01/15/99 1730
CIS-1,2-DICHLOROETHENE < 0.0050 o.ooso mg/1 PAP 01/15/99 1730
CIS-1,3-DICHLOROPROPENE < 0.0050 0.0050 mg/1 PAP 01/15/99 1730
DIBROMOCHLOROMETHANE < 0.0050 0.0050 mg/1 PAP 01/15/99 1730 I
ETHYLBENZENE < 0.0050 0.0050 mg/1 PAP 01/15/99 1730
METHYLENE CHLORIDE < 0.0050 o. 0050 mg/1 PAP 01/15/99 1730
STYRENE < 0. 0050 0 .0050 mg/1 PAP 01/15/99 1730
TETRACHLOROETHENE ' 0 .0050 0.0050 mg/1 PAP 01/15/99 1730 I
TOLUENE < 0.0050 0.0050 mg/1 PAP 01/15/99 1730
TRANS-1,2-DICHLOROETHENE < 0.0050 0.0050 mg/1 PAP 01/15/99 1730
TRANS-1,3-DICHLOROPROPENE < 0.0050 0.0050 mg/1 PAP 01/15/99 1730
TRICHLOROETHENE < 0.0050 0.0050 mg/1 PAP 01/15/99 1730 I
VINYL ACETATE < 0 .010 0. 010 mg/1 PAP 01/15/99 1730
VINYL CHLORIDE < 0 .010 0.010 mg/1 PAP 01/15/99 1730
XYLENE (TOTAL) < 0,0050 0.0050 mg/1 PAP 01/15/99 1730 I
Prop Procedure Method Analyot Prep Date I
Analytical Prep Procedureo:
BNA SEMIVOLATILES SWS46 3500B JMT 01/19/99 1200
DOWTHERM SWB46 35008 JMT 01/19/99 1200 I
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000047 I
Davis & Floyd, Inc. I PO Drawer 428 I Greemvood, SC 29648 I 816 E. Durst Avenue [ Greenwood, SC 29649 I [phone] I fax [phone]
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Df\VIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: EE-58
Matrix
Para.meter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMET~E
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENB
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
BTHYLBENZENE
MBTHYLENB CHLORIDE
STYRBNB
TBTRACHLOROETHENB
TOLUENE
TRANS-1,2-DICHLOROETHENB
TRANS-1,3-DICHLOROPROPBNE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
GW/ChemW
'
'
'
'
'
<
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
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NC Certification Number: 25
'
Project Number: 60885.00
Report Date
Page 1 of 1
February 01, 1999
R••ult
0.0050
0 .0050
0 . 0050
0.0050
0. 0050
0.0050
0. 0050
0. 010
0. 010
0.0050
0. 010
0.0050
o.ooso
0.0050
0.010
0.0050
0.0050
0.0050
0.010
0.0050
0. 010
0 . 0050
0 . 00S0
0. 0050
0 .0050
0 .0050
0 .0050
0 .0050
0 . 0050
0 .0050
0 .0050
0.0050
0.010
0.010
0.0050
Sample ID L99011502-14
Date Collected: 14-JAN-99 13:44
Date Received: 14-JAN-99
Qual RDL Unite
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0 .0050 mg/1 PAP
0 .0050 mg/1 PAP
0.0050 mg/1 PAP
0.010 mg/1 PAP
0.010 mg/1 PAP
0.0050 mg/1 PAP
0.010 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.010 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.010 mg/1 PAP
0.0050 mg/1 PAP
0.010 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0. 0050 mg/1 PAP
0.0050 mg/1 PAP
0 .0050 mg/1 PAP
0 .0050 mg/1 PAP
0.0050 mg/1 PAP
0. 0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0. 010 mg/1 PAP
0.010 mg/1 PAP
0.0050 mg/1 PAP
000018
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
~1/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/1S/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
01/15/99
Time
1750
1750
1750
1750
1750
1750
17_50
1750
1750
1750
1750
1750
1750
1750
1750
1750
1750
1750
1750
1750
1750
l 750
17S0
1750
1750
1750
1750
1750
1750
1750
1750
1750
1750
1750
1750
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
D!\YIS
FLtiYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC,
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: T-35
Matrix
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROM STHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENB
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
GW/ChemW
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NC Certification Number: 25
'
· Raault
o.ooso
0.0050
0.0050
0.0050
0.0050
0 .0050
0. 0050
0.010
0.010
0.0050
0. 010
0.0050
0.0050
0 .0050
0. 010
0.0050
0,0050
0.0050
0.010
0.0050
0.010
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
o.ooso
0.0050
0. 010
0. 010
0.0050
Project Number: 608B5.00
Report Date
Page 1 of 1
: February 01, 1999
Sample ID L99011502-15
Date Collected: 14-JAN-99 14:37
Date Received: 14-JAN-99
Qual RDL Onita Analyst Date
0 .0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0 .0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0 .010 mg/1 PAP 01/19/99
0 .010 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0. 010 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0. 0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0. 010 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.010 mg/1 PAP 01/19/99
0.0050 mg/1 PAP .01/19/99
0. 010 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0 .0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/~9
0. 0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0 .0050 mg/1 PAP 01/19/99
0 .0050 mg/1 PAP 01/19/99
0 .0050 mg/1 PAP 01/19/99
0. 0050 mg/1 PAP 01/19/99
0.010 mg/1 PAP 01/19/99
0. 010 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
000043
Timo
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
1733
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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Di\YIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JSRRY MCMURRAY
Client ID: TRIP BLANK
Matrix
Parameter
Volatile Organica
SW846 B260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONB
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANB
BROMOFORM
BROMOMBTHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBBNZENB
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-0ICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TR.ANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
GW/cherow
<
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<
<
<
<
<
NC Certification Number: 25
'
Result
0 .0050
0. 0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.010
0.010
0.0050
0.010
0 .0050
0. 0050
0.0050
0.010
0.0050
0.0050
0.0050
0.010
0.0050
0.010
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.010
0.010
0.0050
Project Number: 60885.00
Report Date
Page 1 of 1
: February 01, 1999
Sample ID L99011502-16
Date Collected:
Date Received: 15-JAN-99
Qual RDL Onita
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0. 0050 mg/1 PAP
0 . 0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0 .010 mg/1 PAP
0 .010 mg/1 PAP
0.0050 mg/1 PAP
0.010 rng/1 PAP
0.0050 mg/1 PAP
0. 0050 mg/1 PAP
0.0050 mg/1 PAP
0.010 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.010 mg/1 PAP
0.0050 mg/1 PAP
0. 010 mg/1 PAP
0.0050 mg/1 PAP
0. 0050 mg/1 PAP
0 .0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 rng /1 PAP
0.0050 mg/1 PAP
0. 0050 mg/1 PAP
0 ,0050 mg/1 PAP
0 . 0050 mg/1 PAP
0 .0050 mg/1 PAP
0.010 mg/1 PAP
0.010 . mg/1 PAP
0.0050 mg/1 PAP
000050
Time
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
~1/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19 /99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
01/19/99 1714
Davis & Floyd, Inc. I PO Drawer 428 ] Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
Di\YIS
FLOYD LABORATORY ANALYSIS REPORT
Method Conformance Summary
Client: HNA HOLDINGS, INC.
Login: L990 I I 502
Project Number: 60885.00
Report Date: February I, I 999
Semi
Criteria Volatiles Volatiles Metals
Sample Holding Time ✓ ✓ NIA
Standards Preparation ✓ ✓ NIA
Instrument Tuning ✓ " NIA
Instrument Calibration " " NIA
Calibration Verification " " NIA
Degradation Check NIA NIA NIA
Interference NIA NIA NIA
Sample/Standard
Blanks Results ✓ ✓ NIA
Method Accuracy ✓ " NIA
Method Precision ✓ " NIA
Surrogate Recovery " " NIA
PDS/SD/MSA NIA NIA NIA
TCLP Preparation NIA NIA NIA
Key ✓ = Met Criteria Met
NIA = Not Applicable
• = Method Criteria Not Met• Seefootnote(s) below.
PDS = Post Digestion Spike
SD = Serial Dilution
MSA = Method of Standard Additions
Footnotes: TOC analyses are performed in the inorganics area.
Inorganics Other
✓ NIA
✓ NIA
NIA NIA
✓ NIA
✓ NIA
NIA NIA
NIA NIA
✓ NIA
✓ NIA
✓ NIA
NIA NIA
NIA NIA
NIA NIA
"Spike Added" amounts are given in ug/L on Volatile and Semi-volatile "Matrix
Spikes and Duplicates" and Laboratory Control Standard and Duplicates"
summaries.
Prepared by~{
000051
'
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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FLtlYD
Method Blanks
Blank
Parameter
Volatile Organics
SWB46 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TBTRACHLOROETHANE
1,1,2-TRICHLOROETHANB
1,1-DICHLOROETHANE
1,1-DICHLOROETHENB
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-MIITHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANB
BROMOFORM
BROMOMETHA.NE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBBNZBNE
CHLOROETHANE
CHLOROFORM
CHLOROMETHA.NB
CIS-1,2-DICHLOROETHENB
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROBTHENB
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
MB1586B:1
LABORATORY ANALYSIS REPORT
Report Date January 28, 1999
Page l of l
Matrix GW/ChemW
WorkGroup: WG15868
Cone Qual RDL O'nite J>.naly•t Date Time
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.010 0.010 mg/1 PAP 01/15/99 0934
' 0.010 0.010 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.010 0.010 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0. 010 0.010 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0. 010 0.010 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.010 0. 010 mg/1 PAP 01/15/99 0934
' o.ooso 0 .0050 mg/1 PAP !)1/15/99 0934
' 0.0050 0 . 0050 mg/1 PAP 01/15/99 0934
' 0.0050 o. 0050 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
' o.0050 0.0050 mg/1 PAP 01/15/99 0934
' 0.010 0.010 mg/1 PAP 01/15/99 0934
' 0. 010 0.010 mg/1 PAP 01/15/99 0934
' 0.0050 0.0050 mg/1 PAP 01/15/99 0934
000052
Davis & Floyd, Inc. l PO Drawer 428 1 Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 ! (864) 229•4413 I Fax (864) 229•7119
DAYIS
FLt1YD
Method Blanks
Blank : MB15880:1
Parameter
Volatile Organics
SW846 8260B
1,1,l·TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETI-W'lE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANB
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
LABORATORY ANALYSIS REPORT
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
'
Cone
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.010
0.010
0.0050
0.010
0.0050
0.0050
0. 00 so
0. 010
0.0050
0.0050
0.0050
0. 010
0.0050
0.010
0 .0050
0.0050
0.0050
0.0050
0.0050
0 .0050
0.0050
0.0050
0.0050
0.0050
0.0050
0. 010
0. 010
0.0050
Report Date
Page 1 of 1
: February 10, 1999
Matrix GW/ChemW
WorkGroup: WG15880
Qual RDL Units Analyet Date
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0 . 0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.010 mg/1 PAP 01/19/99
0.010 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0. 010 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.010 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.010 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.010 mg/1 PAP ,01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0 . 0050 mg/1 PAP 01/19/99
0. 0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0. 010 mg/1 PAP 01/19/99
0.010 mg/1 PAP 01/19/99
0.0050 mg/1 PAP 01/19/99
0000~3
Time
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
0950
Davis & rloyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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FLt1YD
Method Blanks
Blank : MB15919:l
Para.meter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENB
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DlCHLOROPROPENE
TRICHLOROETHENE
VINYL ACETJ..TE
VINYL CHLORlDE
XYLENE (TOTAL)
LABORATORY ANALYSIS REPORT
Report Date ' February 10, 1999
Page 1 of 1
Matrix GW/ChemW
WorkGroup: WG15919
Cone Qual RDL Onita Analyst Date Time
< 0.0050 0 .0050 mg/1 PAP 01/20/99 0844
< 0.0050 o. 0050 mg/1 PAP 01/20/99 0844
< 0.0050 0.0050 mg/1 PAP 01/20/99 0844
< 0.0050 0.0050 mg/1 PAP 01/20/99 0844
< 0 . 0050 0.0050 mg/1 PAP 01/20/99 0844
< 0.0050 0.0050 mg/1 PAP 01/20/'J9 0844
< 0.0050 0.0050 mg/1 PAP 01/20/99 0844
< 0.010 0. 010 mg/1 PAP 01/20/99 0844
< 0.010 0.010 mg/1 PAP Ol/20/9'J 0844
< o.ooso 0.0050 mg/1 PAP 01/20/99 0844
< 0.010 0.010 mg/1 PAP 01/20/99 0844
< 0.0050 0.0050 mg/1 PAP 01/20/99 0844
< 0.0050 0.0050 mg/1 PAP 01/20/99 0844
< 0.0050 0.0050 mg/1 PAP 01/20/99 0844
< 0.010 0. 010 mg/1 PAP 01/20/99 0844
< 0.0050 0.0050 mg/1 PAP 01/20/'J9 0844
< 0.0050 0.0050 mg/1 PAP 01/20/99 0844
< o.ooso o.ooso mg/1 PAP 01/20/99 0844
< 0. 010 0.010 mg/1 PAP 01/20/99 0844
< 0.0050 0.0050 mg/1 PAP 01/20/99 0844
< 0.010 0.010 mg/1 PAP. 01/20/99 0844
< o.ooso 0.0050 mg/1 PAP 01/20/99 0844
< 0.0050 0.0050 mg/1 PAP 01/20/99 0844
< 0.0050 0.0050 mg/1 PAP 01/20/99 0844
< 0.0050 0.0050 mg/1 PAP 01/20/';19 0844
< o.ooso 0.0050 mg/1 PAP 01/20/99 0844
< 0.0050 0.0050 mg/1 PAP 01/20/99 0844
< 0.0050 0.0050 mg/1 PAP 01/20/99 0844
< 0.0050 0.0050 mg/1 PAP 01/20/99 0844
< 0.0050 0.0050 mg/1 PAP 01/20/99 0844
< 0.0050 0.0050 mg/1 PAP 01/20/99 0844
< 0.0050 0.0050 mg/1 PAP 01/20/99 0844
< 0.010 0.010 mg/1 PAP 01/20/99 0844
< 0.010 0.010 mg/1 PAP 01/20/99 0844
< 0.0050 0.0050 mg/1 PAP 01/20/99 0844
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 ] 816 E. Durst Avenue I Greenwood, SC 29649 ] [phone] 1 fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS LCS15868:l
1,1-DICHLOROETHENE 20.00 0.0197
BENZENE 20. 00 0.019B
CHLOROBENZENB 20.00 0. 0194
TOLUENE 20 00 0.0197
TRICHLOROETHENE 20.00 0. 0197
Report Date
Page 1 of 1
January 2B, 1999
Matrix GW/ChemW
WorkGroup: WG1586B
Method SW846 82608
98.3 70-1-26
98.9 85-121
96.B B2·119
98.5 83-122
98.5 81-122
000055
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 l [phone] \ Fax [phone]
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Df\YIS
FLOYD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
: LCSl5919:l
20.00
20.00
20.00
20.00
20. 00
21. 91
20. 77
20.29
20. 63
20.09
Report Date
Page 1 of 1
January 28, 1999
Matrix GW/ChemW
WorkGroup: WG15919
Method SWB46 8260B
109.6
103.9
101.s
103.2
100. 5
70-126
B5-121
82-119
83-122
81-122
00000C
Davis & Floyd, Inc. I PO Drawer 428 1 Greenwood, SC 29648 I 816 E. Durst Avenue ! Greenwood, SC 29649 I [phone] I Fax [phone]
Df\YIS
FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
i{{i1ii:Jf[::/j:}:ii.·}>·•: . -.
1,1-DICHLOROBTHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
MS9901150l-Ol:15B68
MSD99011501-0l: 1_5868
i·::H;_if~
:':./~d_d_ll4
50.00
50.00
50.00
SO.OD
50.00
50.00
50. 00
50.00
50.00
so. 00
Report Date
Page 1 of 1
January 28, 1999
Matrix GW/Chemw
WorkGroup: WG15868
Method SWB46 82608
:xs~~Pi~\9\ \t,tS\J/ =·-=--·,. :t,ia :>i/::Lf~ita
/~.?.bft /:t)/(~J.~-~·t:-::·: :"":-;-}\2'.ic'.C'·.··. •,•,_:_ >\~·~£1
< 0.00500 0.0478
< 0.00500 0.0472
< 0.00500 0.0477
< 0.00500 0.0492
< 0,00500 0.0486
0.0493
0.0507
0.0501
0. 0513
0,0506
98, 7
101. 4
100.2
102.7
101.2
000057
95.S
94.S
95.3
98.4
97 .2
3.23
7.13
4.99
4.24
3.99
74-125
83-123
82-120
84-120
83-123
12
10
12
10
11
74-125
83-123
82-120
84-120
B3-123
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 \ [phone] I Fax [phone]
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Di\YIS
FLo'YD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
/:/::.\}\}_:-..;:-:::\::::-.·
.,,.:_."p~-r~m~te_r
1,1-DICHLOROETHENE
BBNZENB
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENB
Report Date January 28, 1999
MS99011S02-15:15880
MSD99011502-l5:l5880
Page 1 of
Matrix
WorkGroup:
Method
1
GW/ChernW
WG15880
SW846 8260B
.'.(~P;~_k:~ ':?/~a:~pie-: :-rMs·/·= ' · -·=··.:::.,Ms
· :;:_A~d-~_d ./\::\Ut~~ri9:/ =·:r::\rcJ~~:-> 'if:/:.·q:f;· ·Limits
·\{)/;,.·R·E_~(
50.00
50.00
50.00
50.00
50.00
SD.OD
SO.DO
50.00
50.00
50.00
< s.oo
< 5.00
< 5.00
< 5.00
< 5.00
51.24
so. 22
49 .65
49.34
51.05
51. 85
50.68
49. 38
49.66
51.42
102.5
100 .4
99.3
98.7
102.1
000058
103.7
101. 4
98.8
99.3
102.s
1.18
0.912
0.545
0.646
0. 722
74-125
83-123
82-120
84-120
83-123
12
10
12
10
11
74-125
83-123
82-120
84-120
83-123
'
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue \ Greenwood, SC 29649 I {864) 229-4413 \ Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
1,1-DICHLOROBTHENE
BENZENE
CHLOROBBNZENE
TOLUENE
TRICHLOROETHENE
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROBTHENE
MS99011502-06:15919
MS099011502-06:15919
50.00
50.00
50.00
50.00
so.co
50.00
50.00
50.00
so.co
so.co
< 5.00
35.16
33.18
< s.oo
< 5.00
52.70
B5.07
80.52
49.17
51.50
Report Date
Page 1 of 1
: January 28, 1999
Matrix GW/ChemW
WorkGroup: WG15919
Method SWB46 82608
51. 63
85 .15
BO. 97
50.28
50. 62
105.4
99.8
94.. 7
98.3
103.0
103.3
100.
95.6
100.6
101. 2
2.05
0.0940
0.557
2.23
1. 72
74-125
03-123
02-120
84-120
83-123
12
10
12
10
11
74-125
83-123
82-120
84-120
83-123
000059
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 1 816 E. Durst Avenue 1 Greenwood, SC 29649 I {864) 229-4413 j Fax [phone]
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FLOYD LABORATORY ANALYSIS REPORT
Surrogates % Recovery
L9!:I011502-0l
L99011502-02
L990l1502-03
L99011S02-04
L99011502-0S
L99011502-06
L99011502-0B
L99011502-09
L99011502-10
L99011502-ll
L99011502-12
L99011502-14
L99011502-15
L99011502-16
LCS15868:l
MB15868:l
MS99011501-01:15B68
MSD99011501-01:15868
MB15880:1
MS99011502-1S:15BBO
MSD99011502-15:15880
LCS15919:1
MB15919:1
MS99011502-06:15919
MSD99011502-06:15919
Measi.lreDate ·.
15-JAN-99 14:13
15-JAN-99 14:32
15-JAN-99 14:52
15-JAN-99 15:12
15-JAN-99 15 :32
20-JAN-99 17:04
15-JAN-99 16:11
15-JAN-99 16 :31
15-JAN-99 16:50
15-JAN-99 17:10
15-JAN-99 17:30
15-JAN-99 17:50
19-JAN-99 17: 33
19-JAN-99 1 7: 1-4
15-JAN-99 18:09
15-JAN-99 09: 3-4
15-JAN-99 10:56
15-JAN-99 11:16
19·JAN-99 09:50
19-JAN-99 17:53
19-JAN-99 18:13
20-JAN-99 18: -42
20-JAN-99 08: 44
20-JAN-99 17:24
20-JAN-99 17:44
DCB 1,2-DICHLOROETHANE-D4
BFB BROMOFLUOROBENZBNE
TOL TOLUENE-DB
96.7
99.1
98.2
97.6
103.1
107.1
101. 8
105.1
102.8
102.7
104.3
103. 3
99.0
97.3
105. 3
99.8
89.3
96.7
101.1
107.4
111.l
116 .9
102.5
109. 3
113 .1
94 .-4
96.2
89. -4
92.0
93 .9
100 .3
92.3
100.0
100.7
95. 8
92. 0
93.7
92.3
93.0
92.9
91.3
91. 9
93.1
9-4.1
94.2
96.8
94.2
94.2
100.s
101. 0
Report Date
Page 1 of l
Matrix
Method
96.8
96.1
94.6
95.1
95.0
98.2
97.7
93.4
93.8
94.9
93.4
95.3
102.9
101. 9
93.7
94.l
95.6
94.0
101. 6
100. 7
98.5
97.3
99.8
98.4
94.5
000060
January 28, 1999
GW/ChemW
SW846 8260
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] l Fax {864) 229-7119
Dl\YIS
FLOYD
Method Blanks
Blank
Parameter
Selllivolatile Organics
SW846 8270C
1, l' -BIPHENYL
1,2,4-TRICHLOROBENZENE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DICHLOROPHENOL
2,4-DIMETHYLPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2, 6-0IN_ITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-METHYL-4,6-DINITROPHENOL
2-METHYLNAPHTHALENE
2-METHYLPHENOL
2-NITROANILINE
2-NITROPHBNOL
J,3'-DICHLOROBENZIDINE
3-NITROANILINE
4-BROMOPHENYL PHENYL ETHER
4-CHLOR0-3-METHYLPHENOL
MB15912:1
4-CHLOROANI LINE
4-CHLOROPHENYL PHENYL ETHER
4-METHYLPHENOL
4-NITROANILINE
4-NITROPHENOL
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
BENZO(A)ANTHRACENE
BENZO(A)PYRENE
BENZO(B)FLUOR.ANTHENE
BENZO(G,H,I)PERYLENE
BENZO(K)FLUOR.ANTHENE
BENZOIC ACID
BENZYL ALCOHOL
BIPHENYL ETHER
BIS(2-CHLOROETHOXY)METHANS
LABORATORY ANALYSIS REPORT
Report Date February 10, 1999
Page 1 of 2
'
Matrix GW/ChemW
WorkGroup: WG15912
Cone Qual RDL Onita Analyst Date Time
< 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1147
< 0.010 0.010 rng/1 DSD/JRN 01/21/99 1147
< 0.010 0.010 rng/1 DSD/JRN 01/21/99 1147
< 0.010 0.010 rng/1 DSD/JRN 01/21/99 1147
< 0.010 0.010 rng/1 DSD/JRN 01/21/99 1147
< 0.010 0.010 rng/1 DSD/JRN 01/21/99 1147
< 0.010 0.010 rng/1 DSD/JRN 01/21/99 1147
< 0.010 0.010 rng/1 DSD/JRN 01/21/99 1147
< 0. 010 0.010 rng/1 DSD/JRN 01/21/99 1147
< 0.025 0.025 rng/1 DSD/JRN 01/21/99 1147
< 0.010 0. 010 rng/1 DSD/JRN 01/21/99 1147
< 0.010 0.010 rng/1 DSD/JRN 01/21/99 1147
< 0.010 0.010 rng/1 DSD/JRN Ol/21/9'iJ 1147
< 0.010 0 .010 mg/1 DSD/JRN Ol/21/'iJ9 1147
< 0. 025 0 . 025 mg/1 DSD/JRN Ol/21/9'iJ 1147
< 0.010 0. 010 rng/1 DSD/JRN 01/21/99 1147
< 0.010 0 .010 rng/1 DSD/JRN Ol/21/'iJ9 1147
< 0.010 0.010 mg/1 DSD/JRN 01/21/9'iJ 1147
< 0.010 0. 010 mg/1 DSD/JRN Ol/21/9'iJ 1147
< 0.010 0.010 rng/1 DSD/JRN Ol/21/9'iJ 1147
< 0.010 0. 010 rng/1 DSD/JRN 01/21/99 1147
< 0.010 0.010 mg/1 OSD/~RN Ol/21/9'iJ 1147
< 0.010 0.010 mg/1 DSD/JRN Ol/21/'iJ9 1147
< 0.010 0.010 mg/1 DSD/JRN 01/21/99 1147
< 0.010 0 .010 mg/1 DSD/JRN 01/21/99 1147
< 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1147
< 0.010 0.010 mg/1 DSD/JRN 01/21/99 1147
< 0. 025 0. 025 mg/1 DSD/JRN 01/21/99 1147
< 0.010 0 .010 mg/1 DSD/JRN 01/21/99 1147
< 0.010 0 .010 mg/1 DSD/JRN 01/21/99 1147
< 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1147
< 0.010 0.010 mg/1 DSD/JRN 01/21/99 1147
< 0.010 0 .010 mg/1 DSD/JRN 01/21/99 1147
< 0. 010 0. 010 rng/1 DSD/JRN 01/21/99 1147
< 0.010 0 .010 mg/1 DSD/JRN 01/21/99 1147
< 0.010 0 .010 mg/1 DSD/JRN 01/21/99 1147
< 0. 050 0.050 rng/1 DSD/JRN 01/21/99 1147
< 0.010 0.010 mg/1 DSD/JRN 01/21/99 1147
< 0.010 0.010 mg/1 DSD/JRN 01/21/99 1147
< 0. 010 0. 010 mg/1 DSD/JRN 01/21/99 1147
UOOOGl
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FLt1YD
Method Blanks
Blank ' MB1S912:l
Par;uneter
BIS(2-CHLOROETHYL)ETHER
BIS{2-CHLOROISOPROPYL)ETHER
815(2-ETHYLHEXYL)PHTHALATE
BUTYL BENZYL PHTHALATE
CHRYSENB
DI-N-BUTYL PHTHALATE
DI-N-OCTYL PHTHALATE
DIBENZ(A,H)ANTHRACENE
DIBENZOFURAN
DIETHYL PHTHALATE
DIMETHYL PHTHALATE
FLUORANTHENE
FLUORENE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROCYCLOPEN'I'ADIENE
HEXACHLOROETHANE
INDENO(l,2,3-CD)PYRENE
ISOPHORONE
N-NITROSOOI-N-PROPYLAMINE
N-NITROSODIPHENYLAMINE
NAPHTHALENE
NITROBENZENE
PEN'I'ACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRENE
Prep Procedure Method
.Analytical Prep Procedures:
BNA SEMIVOLATILES SW846
DOWTHERM SW846
LABORATORY ANALYSIS REPORT
Report Date February 10, 1999
Page 2 of 2
'
Matrix GW/ChemW
WorkGroup: WG15912
Cone Qual RDL unite Analyst Dat• Time
' 0.010 0.010 mg/1 DSD/JRN 01/21/99 1147
' 0.010 0.010 mg/1 DSD/JRN 01/21/99 1147
' 0.010 o. 010 mg/1 DSD/JRN 01/21/99 1147
' 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1147
' 0.010 0.010 mg/1 OSD/JRN 01/21/99 1147
' 0.010 0.010 mg/1 OSD/JRN 01/21/99 1147
' 0.010 0.010 mg/1 DSD/JRN 01/21/99 1147
' 0.010 0. 010 mg/1 DSD/JRN 01/21/99 114 7
' 0.010 o. 010 rng/1 DSD/JRN 01/21/99 1147
' 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1147
' 0.010 0.010 mg/1 DSD/JRN 01/21/99 1147
' 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1147
' 0.010 0 .010 mg/1 DSD/JRN 01/21/99 1147
' 0.010 0 .010 mg/1 DSD/JRN 01/21/99 1147
' 0.010 0.010 mg/1 DSD/JRN 01/21/99 1147
' 0. 010 0. 010 mg/1 DSD/JRN 01/21/99 1147
' 0 .010 0. 010 rng/1 DSD/JRN 01/21/99 1147
' 0.010 0.010 mg/1 DSD/JRN 01/21/99 1147
' 0 .010 0. 010 rng/1 DSD/JRN 01/21/99 1147
' 0 . 010 0.010 mg/1 DSD/JRN 01/21/99 1147
' 0.010 0. 010 mg/1 DSD/JRN 01/21/99 1147
' 0.010 0.010 mg/1 oso/JRN 01/21/99 1147
' 0. 010 0.010 mg/1 DSD/JRN 01/21/99 1147
' 0.025 0.025 mg/1 DSO/~RN 01/21/99 1147
' 0.010 0.010 mg/1 DSD/JRN 01/21/99 1147
' 0.010 0.010 mg/1 OSD/JRN 01/21/99 1147
' 0. 010 0.010 mg/1 DSD/JRN 01/21/99 1147
Analyst Prep Data
3500B JMT 01/19/99 1200
3500B JMT 01/19/99 1200
000062
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
Df\YIS
FLOYD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
Report Date ' January 28, 1999
Page 1 of 1
Matrix GW/Chemw a
'
LCS LCS15!112:l WorkGroup: WG15912
Method SW846 B270C
1,2,4-TRICHLOROBENZENE 50.00 33.21 66. 4 20-103
1,4-DICHLOROBENZENS 50.00 32.01 64.0 18-99
2,4-DINITROTOLUENE 50.00 43.27 86 5 39-115
2-CHLOROPHENOL 75.00 52.62 70.2 27-109
4-CHLOR0-3-METHYLPHENOL 75.00 58.04 77 .4 43-108
4-NITROPHENOL 75.00 22.04 29. 4 o-es
ACENAPHTHENE 50 .00 35. 75 71. 5 43-104
N-NITROSOOI-N-PROPYLAMINE 50 .00 36 .15 72 .3 32-116
PENTACHLOROPHENOL 75 00 38. 20 50.9 1-107
PHENOL 75 .00 25.93 34.6 D-78
PYRENE 50.00 39.23 78 .5 46-119
1,1'-BIPHENYL so.co 38.54 77 .1 15-130
BI PHENYL ETHER 50.00 39 .26 78. 5 25-114
000063
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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FLOYD LABORATORY ANALYSIS REPORT
Malm: Spikes and DuplicaJes
·:::·::, . .-.'."-::'.fi,':">":'i.':. _:.
: P~i~~.e-~~f:
MS/MSD
1,2,4-TRICHLOROBENZENE
1,4-0ICHLOROBENZENE
2,4-DINITROTOLUENE
2-CHLOROPHENOL
4-CHLORO-J-METHYLPHENOL
4-NITROPHENOL
ACENAPHTHENE
N-NITROSODI-N-PROPYLAMINE
PENTACHLOROPHENOL
PHENOL
PYRENE
1, 1' -BIPHENYL
BIPHENYL ETHER
1,2,4-TRICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4-DINITROTOLUENE
2-CHLOROPHENOL
4-CHLOR0-3-METHYLPHENOL
4-NITROPHENOL
ACENAPHTHENE
N-NITROSODI-N-PROPYLAMINE
PENTACHLOROPHENOL
PHENOL
PYRENE
1, 1' -BI PHENYL
BIPHENYL ETHER
Report Date
Page 1 of 1
January 2B, 1999
Matrix GW/ChemW
MS99011502-08:15912
MSD99011502-DB:15912
WorkGroup: WG15912
Method
,. :;.:,:,t_SP\f;(\ -:-·:,::<:/i:i"ample_Tf>·: "MS>t-:· ·. =·-=
\,'A~~-~~{-·-. :/)\(C~~c\_ -i::: /:: :::::c:~~·/:-:-:.:.
SO.OD
so.co
50.00
75.00
75. 00
75.00
50,00
SO.DO
75.00
75.00
SO.OD
50.00
SO.OD
so.co
50. 00
SO.OD
75.00
75,00
75.00
50.00
50.00
75.00
75. 00
50.00
50.00
50.00
' lO. 00 )2.38
' 10. 00 31.!14
' 10.00 37.92
' 10.00 so. 34
' 10.00 56.06
' 25.00 11.67
' 10.00 34.71
' 10 .00 34.64
' ,S, 00 19,79
' 10 .00 22.97
' 10 .00 36.78
' 10.00 38. 24
' 10.00 38. 42
32.10 64.2
31. 79 63.6
40. 02 80.0
49. 34 65.8
55. 47 74.0
17. 45 23.3
34 .21 68,4
34. 77 69.5
32,62 43.5
23 .11 30.8
34.56 69.1
37.86 75. 7
38. 24 76.5
000061
SWB46 B270C
·Ms·.::: ..... · "ii~i-tn
i\R:~'.~/:(-.· ->::\k~'~·:
64.8 15-112
63 ., 17-102
7S. 8 30-123
67.1 15-112
74. 7 25-127
15.6 0-104
69.4 25-122
69.3 24-119
26 .4 9-120
30.6 D-101
73.6 37-123
76.5 21-122
76.8 14-111
0.868 40
0. 471 49
5.39 27
2.01 36
1.06 28
3.9. 7 41
1. 45 32
0. 375 35
49.0 40
0.608 48
6.22 29
0.999 39
0.470 67
15-112
17-102
30-123
15-112
25-127
D-104
25-122
24-119
9-120
D-101
37-123
21-122
14-111
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 [ 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax {864) 229-7119
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Surrogates % Recovery
Report Date January 28, 1999
Page 1 of 1
Matrix GW/ChemW
Method SWB46 3550/8270
L99011502-0B 21-JAN-99 13:06 83.1 83.4
L99011502·09 22-JAN-99 19:49 83.8 51.4
L99011502-10 21-JAN-99 14:25 78.6 76.5
L99011502-ll 21-JAN-99 15:04 76.7 74.7
L99011502-12 21-JAN-99 15:43 71.6 67.3
LCS15912:l 21-JAN-99 12:27 77 .4 77.1
MB15912:l 21-JAN-99 11 :47 78 ., 78.5
MS99011502-08: l 5912 21-JAN-99 lB :20 75. 2 71. 8
MSD99011502-08:15912 21-JAN-99 18:59 74.1 72.0
FBP 2-FLUOROBIPHENYL
NBZ NITROBENZENE·D5
000065
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] j Fax [phone]
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FLO\'D LABORATORY ANALYSIS REPORT
Surrogates % Recovery
L99011502-0B
L99011502-09
L99011502-09
L99011502-10
L99011502·11
L99011502-12
LCS15912:l
MB15912:1
MS99011502-08:15912
MS099011502-0B:15912
TBP 2,4,6-TRIBROMOPHENOL
FBP 2-FLUOROBIPHENYL
2FP 2-FLUOROPHENOL
NBZ NITROBENZENE-05
PHL PHENOL-OS
TPH TERPHENYL-D14
MeasureDate
21-JAN-99 13: 06
22-JAN-99 20:26
21-JAN-99 13:46
21-JAN-99 14:25
21-JAN-99 15:04
21-JAN-99 15: 43
21-JAN-99 12 :27
21-JAN-99 11: 4 7
21-JAN-99 18: 20
21-JAN-99 18 : 59
73 .4 73.6
67.6 85.0
83.9 56.2
78.8 69.3
74.0 67. 8
70.2 63.3
75.6 68.S
74.5 69.1
68.1 66.3
70.7 65.7
Report Date
Page 1 of 1
January 28, 1999
Matrix
Method
45. 7
39,6
40. 6
43.2
42. 7
37. 2
45. 7
45. 9
40. 5
40 . 8
GW/ChemW
SWB46 8270
NBZ :·PHL
26:-1'()9 D-70
79. 2 34.5
80.7 35.8
98.3 33.8
72.5 33.1
70.9 32.4
63.9 28.2
73.1 34.4
74.S 34.2
68.2 30 .1
68.3 30. 6
00006G
TPH
.·3S~u·o'/.
76.5
Bl. 3
73.6
72,2
71.5
70.5
77.8
78.7
72.2
68.1
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DL\VIS
FLOYD
Method Blanks
Wet Chemistry
SWB46 9060
Blank
ORGANIC CARBON, TOTAL
: MB15895:1
LABORATORY ANALYSIS REPORT
Report Date January 28, 1999
Page 1 of 1
Matrix GW/ChemW
WorkGroup: WG15895
Cone Qual RDL Uni ta Analy■t Date Tim•
1.0 mg/1 TRB 01/18/99 1555
000067
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 l {864) 229-4413 I Fax {864) 229-7119
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FLt1YD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS LCS1589S:l
'>t:11f :i~ti~-..
ORGANIC CARBON, TOTAL
Report Date
Page 1 of 1
Matrix
January 28, 1999
GW/ChemW
WorkGroup: WG15895
Method SW846 9060
:'"j~f~~-;:,r· ·· i/f).t\•: :: = ,.=·L·cs>= -=-.,., .. ,:,,,,,,-,·:'i.i~i-t=;·='·
:·. Ad~ii_d /(COj1C t? ( i:·\i\\~'fl-: i(i}:((:}{i~'h';.//':-' ·-
10.00 10.90 109.0 90-110
000068
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue ] Greenwood, SC 29649 I {864) 229-4413 I Fax [phone]
DAYIS
FLtfYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
ORGANIC CARBON, TOTAL
MS99011503-0l:15895
MSD99011503-0l:15895
20.00 20. 30
Report Date
Page 1 of 1
: January 28, 1999
Matrix GW/ChemW
WorkGroup: WG15895
Method SW846 9060
91.8 4.81 11 74-132
000063
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] ! Fax {864) 229-7119
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FLOYD LABORATORY ANALYSIS REPORT
Sludge (Reporting Level 3)
000070
Davis & Floyd, Inc. I PO Drawer 428 ! Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 j [phone] I Fax [phone]
DAYIS
FLtlYD LABORATORY ANALYSIS REPORT
January 29, 1999
JERRY MCMURRAY
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
:L99011502
:60885.00
Login Number
Project Number
Description :SLUDGE ANALYSIS -TCLP
Dear Jerry Mcmurray:
We are pleased to provide the enclosed analytical results for the samples received by
Davis & Floyd, Inc. on January 14, 1999.
A formal Quality Assurance/Quality Control program is maintained by Davis & Floyd,
which is designed to meet or exceed the EPA or appropriate regulatory requirements.
All analytical analyses for this project met QA/QC criteria unless otherwise stated in the
footnotes. This report is to be reproduced only in full.
Feel free to contact our Client Services ReIJresentative at [phone] if further
explanation of the analysis is required. Unless other arrangements have been made, samples
will be disposed of or returned 14 days from the date of the report. We appreciate the
opportunity to provide services to your firm.
~X'Vfl':'. F/4NC
h,f~}f'&
Laboratory Manager
000071
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone] I
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Df\VIS
FLtfYD LABORATORY ANALYSIS REPORT
Master Tracking List
Client
Contact
Sample ID
S 46 8260B
L99011S02-02
tt(i!i~;'.¥i::::': .,.
Volatile Organic
SW846 8260B
Volatile Organics
SW846 8260B
Volatile Organics
SWB46 8260B
L99011502-05
Volatile Organic•
SW846 8260B
Wat Chemistry
SWB46 9060
L99011502-06
HNA HOLDINGS INC,
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
client ID
HH-77
HH-77 DOP,
-48
ITEF
:n:ntt~7~6J{\:I :'f:'i:::::t)t(/JI:\/Mtf
Volatile Organics //
SW846 8260B /
Wot Chemie~/
/ SWB46/9060
./
L99011502-07 SBR SLUDGE
Pe•ticide• and Herbicide■ TCLP
SW846 1311/BOBlA
SW846 1311/BlSlA
NC Certification Number: 25
Project Number: 60885.00
Report Date
Page l of 3
January 29, 1999
Oat• Collected Date Received
14-JAN-99 10:01 14-JAN-99
01/15/99 1413
14-JAN-99 10:01.
14-JAN-99 10;
01/15/99 1452
01/15/99 1512
-JAN-99 11:01 14-JAN-99
01/15/99 1532
9 1235
01/20/99 1704
01/18/99 13-43
l4-JAN-99 11:01 1-4-JAN-99
01/26/99 1809
01/22/99 1928
000072
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 j 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLO\'D LABORATORY ANALYSIS REPORT
Master Tracking List
Client
Contact
Sample ID
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID
Semivolatile Organica TCLP
SW846 1311/B270C
Trace Metals TCLP
SW846 1311
Volatile Organica TCLP
SW846 1311/82608
L99011502-08
8270C
Volatile Organ'ca
SW846 8260B
L990ll502-09
Semivolatile Organics
SWB46 B270C
Volatile Organics
SWB46 8260B
L99011502-10
Semivolatile Organics
SW846 B270C
Volatile Organics
SW846 8260B
L!:19011502-11
Sei:nivolatile
Sh.846
voiat>~~ Organics
SW846 8260B
PEW-1
PEW-4
PEW-4 DUP.
NC Certification Number: 25
Project Number: 60885.00
Report Date
Page 2 of 3
January 29, 1999
Date Collected Date Received
01/25/99 1211
01/19/99 1655
01/20/59 0947
14-JAN-99 11: 01 14-JAN-99
01/21/99 1306
14-JAN-99
01/21/99 1346
01/15/99 1631
14-JAN-99 12:01 14-JAN-99
01/21/99 1425
0 5/99 1650
14-JAN-99 12: 01
01/21/99 1504
01/15/99 1710
000073
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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FLOYD LABORATORY ANALYSIS REPORT
Master Tracking List
Client
Contact
Sampl• ID
L99011502-1:2 :tttt:R;_t·~;J_:m:::::/::::::
Se~ivolatile Organics
HN~ HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
client ID
Sk'B46 a:noc -----------Volatile Organice:----
SW~-~-B·:r60;
-
FP SLUDGE
Pesticides and Herbicides TCLP
SW846 1311/BOBlA
SWB46 1311/BlSlA
Semivolatile Organics TCLP
SWB46 1311./8270C
Trace Metals TCLP
SW846 1311
Volatile Organics TCLP
SW846 13ll/8260B
L99011502-14
SW846 8260B
L990ll502-15
Vol•tile Organics
SW846 8260B
L990ll502-1Ei
SW846 8260B
N,C Certification Number: 25
Project Number: 60885.00
Report Date
Page 3 of 3
Januar1 29, 1999
Date Collected Date .. Received
---1'1/21/99 1543
14-JAN-99 12:01
14-JAN-99 13: 01
14-JAN-99 14: 01
01/15/99 1730
14-J1'.N-9'
01/26/99 2004
Ol/2S/99 1325
01/25/99 1401
01/19/99 1659
01/20/99 1147
14-JAN-99
01/15/99 1750
01/19/99 1714
000071
--..
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Dursl Avenue I Greenwood, SC 29649 l [phone] I Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
NC Certification Number: 25
'
client HNA HOLDINGS INC. Project Number: 60885.00
P.O. BOX 87
SHELBY, NC 28150 Report Date ' January 29, 1999
Contact JERRY MCMURRAY Page 1 of 2
client ID: SBR SLUDGE Sample ID L99011502·07
Date Collected: 14-JAN-99 11 ; 45
Matrix ' Leachate Date Received ' 14-JAN-99
Para.m•t•r Result Qual RDL MCL Onita .Analyst D•t• Time
Peaticid•• and Herbicide• TCLP
SW846 13ll/8081A
CHLORDANE:, TECHNICAL < 0.0050 0.0050 0 .030 mg/1 KLH 01/20/99 0947
ENDRIN < o. 0010 0.0010 0 . 020 mg/1 KLH 01/20/99 0947
HEPTACHLOR < 0.053 0.00050 0.010 mg/1 KLH 01/20/99 0947
HEPTACHLOR EPOXIDE < 0 .00050 0.00050 0.010 mg/1 KLH D1/20/99 0947
LINDANE < 0.00050 0.00050 0. 40 mg/1 KLH 01/20/99 0947
METHOXYCHLOR < 0.0050 0.0050 10.0 mg/1 KLH 01/20/99 0947
TOXAPHENE < 0. 050 0.050 0.50 mg/1 KLH 01/20/99 0947
SW846 1311/BlSlA
2,4,5-TP (SILVEX) < 0.0010 0.0010 1.0 mg/1 KLH 01/20/99 0947
2,4-D < 0.010 0.010 10.0 mg/1 KLH 01/20/99 0947
Semivolatile Organics TCLP
SWB46 1311/B270C
1,4-DICHLOROBENZENE < 0.10 0.10 7.5 mg/1 DSD/JRN 01/20/99 0947
2,4,5-TRICHLOROPHENOL < 0.10 0.10 400 mg/1 DSD/JRN 01/20/99 0947
2,4,6-TRICHLOROPHENOL < 0.10 0.10 2-0 mg/1 DSD/JRN 01/20/99 0947
2,4-DINITROTOLUENE < 0.10 0.10 0.13 mg/1 0S0/JRN 01/20/99 0947
2-METHYLPHENOL < 0.10 0.10 200 mg/1 DSD/JRN 01/20/99 0947
3&4-METHYLPHENOL < 0.10 0.10 200 mg/1 DSD/JRN 01/20/99 0947
HEXACHLOROBENZENE < 0.10 0.10 0.13 mg/1 DSD/JRN 01/20/99 0947
HEXACHLOROBUTADIENE < 0.10 0 .10 0.50 mg/1 DSD/JRN Ol/20/99 0947
HEXACHLOROETHANE < 0.10 o. 10 3.0 mg/1 DSD/JRN 01/20/99 0947
NITROBENZENE < 0,10 0 .10 2.0 mg/1 DSD/JRN 01/20/99 0947
PENTACHLOROPHENOL < 0.25 0.25 100 mg/1 DSD/JRN 01/20/99 0947
PYRIDINE < 0.10 0.10 5. 0 mg/1 DSD/JRN 01/20/99 0947
Trace Metale TCLP
SWB46 1311
ARSENIC, TOTAL < 0.050 0 .050 5.0 mg/1 JSJ 01/20/99 0947
BARIUM, TOTAL < 0.020 0. 020 100 mg/1 JSJ 01/20/99 094 7
CADMIUM, TOTAL < 0.0050 0.0050 1.0 mg/1 JSJ 01/20/99 0947
CHROMIUM, TOTAL < 0.010 0.010 5.0 mg/1 JSJ 01/20/99 0947
LEAD, TOTAL < 0. 050 0. 050 5.0 mg/1 JSJ 01/20/99 0947
MERCURY, TOTAL < 0.00020 0.00020 0.20 mg/1 BDL 01/20/99 0947
SELENIUM, TOTAL < 0.050 0. 050 1.0 mg/1 JSJ 01/20/99 0947
SILVER, TOTAL < 0.010 0.010 5.0 mg/1 JSJ 01/20/99 0947
000075
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 l 816 E. Durst Avenue I Greenwood, SC 29649 \ [phone] I Fax [phone]
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FLOYD
Client
Contact
LABORATORY ANALYSIS REPORT
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
NC Certification Number: 25
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Project Number: 60B85.00
Report Date
Page 2 of 2
client ID: SBR SLUDGE Sample ID
Parameter
Volatile Organic• TCLP
SW846 1311/8:ZG0B
1,1-DICHLOROETHENE
1,2-DICHLOROETHA.NE
2-BUTANONE
BENZENE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROFORM
TETRACHLOROETHENE
TRICHLOROETHENE
VINYL CHLORIDE
Prep Procodure
Analytical Prep Procedures:
ZHE: EXTRACTION
TCLP EXTRACTION
TCLP SEMIVOLATILES
TCLP PESTICIDES
TCLP HERBICIDES
METALS PREP ICP
Method
SW846
SW846
SW846
SW846
SW846
SW846
SW846
<
<
<
<
<
<
<
<
<
Result Qual
o.oso
0.050
0 .10
o.oso
o.oso
o.oso
o.oso
0.050
0. 050
0.10
RDL
0.050
0 .050
0.10
0.050
0.050
0 .050
0 .050
0.050
0.050
0.10
MCL
0.70
a.so
200
a.so
a.so
100 ,.,
0.70
o. 50
0 .20
Analyst Prop Dato
1311 DBC 01/18/99 1500
1311 JMT 01/18/99 1630
1311/3500A JMT 01/20/99 0830
1311/3510C JMT 01/26/99 0730
1311/SlSlA JMT 01/20/99 1500
3010 JSJ 01/19/99 1030
7470A BDL 01/20/99 1200
00007G
Unite Analyst Date Time
mg/1 PAP 01/20/99 0947
mg/1 PAP 01/20/99 0947
mg/1 PAP 01/20/99 0947
mg/1 PAP 01/20/99 0947
mg/1 PAP 01/20/99 05147
mg/1 PAP 01/20/99 0947
mg/1 PAP 01/20/99 0947
mg/1 PAP 01/20/99 0947
mg/1 PAP 01/20/99 0947
mg/1 PAP 01/20/99 0947
Davis & Floyd, Inc. \ PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 l [phone] ! Fax [phone]
Df\YIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: FP SLUDGE
Matrix Leachate
Paraineter
Pe•ticidea and Herbicides TCLP
SW846 1311/BOBlA
CHLORDANE, TECHNICAL
ENDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
LINDANE
METHOXYCHLOR
TOXAPHENE
SW846 1311/BlSlA
2,4,5-TP (SILVEX)
2,4-D
Se~ivolatil• Organics TCLP
SW846 1311/B270C
1,4-DICHLOROBENZENE
2,4,S-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DINITROTOLUENE
2-METHYLPHENOL
3&4-METHYLPHENOL
HEXACHLOROBENZENE
HBXACHLOROBUTADIENB
HBXACHLOROETHANB
NITROBENZBNB
PENTACHLOROPHBNOL
PYRIDINE
Trace Metal• TCLP
SW846 1311
ARSENIC, TOTAL
BARIUM, TOTAL
CADMIUM, TOTAL
CHROMIUM, TOTAL
LEAD, TOTAL
MERCURY, TOTAL
SELENIUM, TOTAL
SILVER, TOTAL
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Result
0.0050
0.0010
O. 00050
0.00050
0.00050
0.0050
0.050
0.0010
0. 010
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.25
0.10
0.050
4.5
0 .0050
0. 050
0.050
0. 00020
0.084
0. 010
N,C Certification Number: 25
X
Project Number: 60885.00
Report Date
Page 1 of 2
: January 29, 1999
Sample ID L99011502-13
Date Collected: 14-JAN-99 12:24
Date Received: 14-JAN-99
RDL MCL Onita Analyst Date Time
0. 0050 0.030 mg/1 KLH 01/20/99 1147
0. 0010 0.020 mg/1 KLH 01/20/99 1147
0.00050 0 .010 mg/1 KLH 01/20/99 1147
0.00050 0 .010 mg/1 KLH 01/20/99 1147
0.00050 0.40 mg/1 KLH 01/20/99 1147
0.0050 10.0 mg/1 KLH 01/20/99 1147
0.050 0.50 mg/1 KLH 01/20/99 1147
0.0010 1.0 mg/1 KLH 01/20/99 1147
0. 010 10.0 mg/1 KLH 01/20/99 1147
0.10 7.5 mg/1 DSD/JRN 01/20/99 1147
0.10 400 mg/1 DSD/JRN 01/20/99 1147
0 .10 2.0 mg/1 DSD/JRN 01/20/99 1147
0.10 0.13 mg/1 DSD/JRN 01/20/99 1147
0.10 200 mg/1 DSD/JRN 01/20/99 1147
0.10 200 mg/1 DSD/JRN 01/20/99 1147
0.10 0.13 mg/1 DSD/JRN 01/20/99 1147
0.10 0.50 mg/1 DSD/JRN 01/20/99 1147
0.10 3.0 mg/1 DSD/JRN 01/20/99 1147
0.10 2.0 mg/1 DSD/JRN 01/20/99 1147
0.25 100 mg/1 DSD/JRN 01/20/99 1147
0.10 5.0 mg/1 DSD/JRN 01/20/99 1147
0.050 5.0 mg/1 JSJ 01/20/99 1147
0.020 100 mg/1 JSJ 01/20/99 1147
0.0050 1.0 1119/l JSJ 01./20/99 1147
0.050 5.0 mg/1 JSJ 01/20/99 1147
0.050 5.0 mg/1 JSJ 01/20/99 1147
0.00020 0.20 mg/1 BDL 01/20/99 1147
0 .050 1. 0 mg/1 JSJ 01/20/99 1147
0 .010 5.0 mg/1 JSJ 01/20/99 1147
000077
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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Di\YIS
FLOYD
Client
Contact
LABORATORY ANALYSIS REPORT
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
NC Certification Number: 25
'
Project Number: 60885.00
Report Date
Page 2 of 2
January 29, 1999
Client ID: FP SLUDGE Sample ID L99011502-13
Para.meter
Volatile organics TCLP
SW846 1311/8260£
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
2-BtrrANONS
BENZENE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROF'ORM
TETRACHLOROETHENE
TRICHLOROETHENE
VINYL CHLORIDE
Prep Procedure
Analytical Prep Procedures:
TCLP EXTRACTION
TCLP SEMIVOLATILES
TCLP PESTICIDES
TCLP HERBICIDES
METALS PREP ICP
Method
SW846
SW846
SW846
SW846
SW846
SW846
<
<
<
<
<
<
<
<
<
<
Qual
0.050
o. 050
0.10
0.050
0. 050
0.050
0.050
0.050
0. 050
0.10
Analyst Prep Date
1311 JMT 01/18/99
1311/3SOOA JMT 01/20/99
1311/3510C JMT 01/26/99
1311/BlSlA JMT 01/20/99
3010 JSJ 01/19/99
7470A BDL 01/20/99
RDL MCL
0 .050 0.10
0 .050 a.so
0.10 200
0.050 a.so
0. 050 a.so
0.050 100
o.oso 6.0
0.050 0.70
0.050 a.so
0.10 0.20
1630
0830
0730
1500
1030
1200
000078
Units Analyst Data Time
mg/1 PAP 01/20/99 1147
mg/1 PAP 01/20/'H 1147
mg/1 PAP 01/20/99 1147
mg/1 PAP 01/20/99 1147
mg/1 PAP 01/20/99 1147
mg/1 PAP 01/20/99 1147
mg/1 PAP 01/20/99 1147
mg/1 PAP 01/20/99 1147
mg/1 PAP 01/20/99 1147
mg/1 PAP 01/20/99 1147
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue [ Greenwood, SC 29649 I [phone] l Fax [phone]
Df\YIS
FLOYD LABORATORY ANALYSIS REPORT
CASE NARRATIVE
Account: HNA Holdings, Inc. -Shelby, NC
Project: 60885.00
Date: February 11, 1999
OVERVIEW
On January 24, 1998, Davis & Floyd received two sludge samples from the plant in Shelby, NC. The samples were
extracted by Method 1311, Toxicity Characteristic Leaching Procedure (TCLP) using the appropriate fluid and
sample vessel. The TCLP extracts were then analyzed for volatile organics, semivolatile organics, trace metals,
pesticides and herbicides. This report contains the analytical data for the following login numbers:
Sample Number
L990 I 1502-07
L99011502-13
Sample ID
SBR Sludge
FP Sludge
The samples were transported to our laboratory on ice accompanied by documented Chain of Custody forms. Upon
receipt by the laboratory, the sample custodian checked samples against the Chain of Custody for agreement and
documented the pH of all preserved sample fractions on the sample login report. All samples were received intact
with no discrepancies noted by the sample custodian.
TRACE METALS
INDUCTIVELY COUPLED PLASMA {ICP)
Sample Analysis
Arsenic, barium, cadmium, chromium, lead, selenium and silver were analyzed by Inductively Coupled Plasma
(ICP) on a Thermo Jarrell Ash 61E simultaneous system according to the procedure described in SW846 Method
6010B. Prior to the analysis, 25 mis ofTCLP extract was digested in an acid matrix according to the sample
preparation procedure described in SW846 Method 3010A. On a daily basis, an initial calibration standard (!CV) at
I 0.0 mg/I (I .0 mg/I Ag) is analyzed. This is followed by an interference check standard (ICSAB) immediately after
the ICY and verified every eight hours thereafter. A continuing calibration verification standard (CCV) is analyzed
after every ten samples for the duration of the analysis. ·
Quality Control
A matrix spike (MS) and matrix spike duplicate (MSD) were analyzed on sample L99011502-13. Matrix spikes,
matrix spike duplicates, and laboratory control samples (LCS) are analyzed on a five percent frequency. All QC
samples met acceptable criteria.
Since the barium results for L99011502-13 were less than 50 times the RDL, a 1/5 serial dilution was performed. It
passed with a 5.1% difference. Also on sample L99011502-13, chromium was more negative than the RDL. A 1:4
dilution was performed and post-spiked (94.8% recovery).
MERCURY COLD VAPOR
Sample Analysis
Both samples were digested and analyzed for mercury on a Perkin-Elmer FIMS 100 system according to the
procedure described in SW846 Method 74 70A. Initial calibration consists of a linear regression curve of a blank
and six standards. Prior to analysis and on a ten percent frequency thereafter the curve is verified with a blank
00007B
Davis & Floyd, Inc. I PO Drawer 428 1 Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] l Fax [phone]
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FLtfi'D LABORATORY ANALYSIS REPORT
(JCB/CCB) and a standard (!CV/CCV). Agreement must be,within ten percent of the true value for the !CV and
first CCV. A twenty-percent agreement is for all subsequent CCV's.
Quality Control
A matrix spike and matrix spike duplicate were analyzed on sample L99011502-13. An extraction blank was also
analyzed.
For every set of twenty samples a method blank, matrix spike, matrix spike duplicate, and a LCS must be analyzed.
For every ten samples a sample duplicate is analyzed. All QC samples fell within acceptable criteria.
VOLATILE ORGANICS
Sample Analysis
The samples and any associated QC were prepared and analyzed according to the procedure described in SW846
Method 8260B. The samples were analyzed at ambient temperature on instrument HP5972A, a Hewlett Packard
5972 GC/MS equipped with an OI purge and trap system using a 5 ml purge volume. An initial five-point
calibration is performed covering a range of 5 µg/1 to 200 µg/1. For each compound with less than 15% RSD, the
relative response factor is assumed to be constant over the calibration range, and the average response is used for
quantitation. If the ¾RSD is greater than fifteen percent, then linear regression is used for quantitation. Calibration
is verified every twelve hours by checking the GC/MS tuning criteria using 50 ng of BFB and analyzing a
continuing calibration standard at 50 µg/1 and a method blank.
Quality Control
Each sample including QC samples and blanks are spiked with surrogate standards at the 50 µg/l level. All
surrogate recoveries were within the acceptance criteria.
A matrix spike, matrix spike duplicate, and a LCS are analyzed at a minimum frequency of five percent for each
matrix. An matrix spike and matrix spike duplicate were analyzed on both samples. All recoveries on MS, MSD and
LCS analyses were within QC acceptance criteria.
SEMIVOLATILE ORGANICS
Sample Analysis
The samples and any associated QC were analyzed according to the procedure described in SW846 8270C. Prior to
analysis, all samples were extracted by separatory funnel shake out with methylene chloride according to SW846
Method 3510C. The GC/MS analysis was performed on instrument HP5972P, a Hewlett Packard 5972 series
system. An initial five-point calibration is performed covering a range of IO ug/1 to 120 ug/1. For each compound
with less than 15% RSD, the relative response factor is assumed to be constant over the calibration range, and the
average response is used for quantitation. If the ¾RSD was greater than fifteen percent for any compound, the
summation technique was used for quantitation. The correlation for pentachlorophenol would have been 0.962 if
the calibration curve technique had been used. Calibration is verified every twelve hours by checking the GC/MS
tuning criteria using 50 ng of DFTPP and analyzing a continuing calibration standard at 60 µg/1 and a method blank.
Due to the additional parameters required, multiple analyses were required in the analysis of the serrii-volatile
organics.
Quality Control
Each sample including QC samples and blanks is spiked with surrogate standards at a concentration of 50 µg/1 for
the base-neutral compounds and 75 µg/1 for the acid extractable compounds. All surrogate recoveries were within
acceptable limits. A matrix spike and matrix spike duplicate were analyzed at a minimum frequency of five
percent. The matrix spike and matrix spike was performed on both samples. The matrix spike, matrix spike and
LCS met all acceptance criteria.
2 000080
Davis & Floyd, Inc. ! PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] l Fax [phone]
Dl\VIS
FLOYD
GAS CHROMATOGRAPHY
PESTICIDES
Sample Analysis
LABORATORY ANALYSIS REPORT
Prior to analysis, all samples were extracted by separatory funnel shake out with methylene chloride according to
SW846 Method 35 l0C. The GC analysis was performed on a Varian 3400 series system designated as.YARK. An
initial five-point calibration was performed prior to analysis of samples and evaluated using linear regression. The
relative standard deviation met the linearity requirements of the method. Calibration is verified daily by analyzing a
continuing calibration standard.
The samples were originally extracted on January 20, 1999 and given the batch root name of0120XP. Several
targets failed low on the LCS. The samples were re-tumbled. The samples were re-extracted and re-analyzed on
January 26, 1999 and designated as batch root 0126XP.
Quality Control
Each sample including QC samples and blanks are spiked with decachlorobiphenyl (DCB) and tetrachloro-m-xylene
(TCMX) at a concentration of 1.0 µg/1 as the surrogate standard. All surrogate recoveries were within acceptable
limits. A matrix spike and matrix spike duplicate were analyzed on both samples. A LCS was analyzed at a
minimum frequency often percent. All criteria on the QC samples were met. Endrin failed high (19 vs. 15%) on the
ending CCV standard. The data was accepted because no endrin was detected in the samples above the RDL and
any bias would be slightly high based upon the recovery of endrin in the ending CCV.
HERBICIDES
Sample Analysis
Prior to analysis, all samples were extracted by separatory funnel shake out with diethyl ether according to SW846
Method 8151A. The GC analysis was performed on a Varian 3400 series system designated as VARE. An initial
five-point calibration was performed prior to analysis of samples and evaluated using linear regression. The relative
standard deviation met the linearity requirements of the method. Calibration is verified daily by analyzing a
continuing calibration standard.
Quality Control
Each sample including QC samples and blanks are spiked with 2,4-dichlorophenylacetic acid (DCAA) at a
concentration of 2.0 µg/1 as the surrogate standard. Sample L99011502-13 recovered below the acceptable range.
This sample was re-injected on January 25, 1999. Acceptable surrogate recovery was obtained on the second
analysis of the sample. The failure observed in the initial analysis was considered to be due a faulty autosampler
injection. All targets were less than the reporting limits on both analyses of this sample. The original results are
reported. All other surrogate recoveries were within acceptable limits. A matrix spike and matrix spike duplicate
were analyzed on both samples. A LCS was analyzed at a minimum frequency often percent. All criteria on the
QC samples were met.
3 000081
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] \ Fax {864) 229-7119
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INSTRUMENT QC ASSESSMENT SUMMARY
FOR EPA METHOD 6010B
For Samples: lab ID #L99011502-07 lab ID# ____ _ lab ID# ------
lab ID #L98011502-13 lab ID# lab ID# ------

-
-
-
-
-
-
lab ID# _____ lab ID# ____ _ lab ID# ------
lab ID# _____ lab ID# ____ _ lab ID# ------
CRITERIA PIF COMMENTS
INITIAL CALIBRATION: (at least one std and blk daily) p Date of calibration: 1/J 9/99.
1/20/99
All standards and solutions prepared/utilized within method required
holding times p
Cal Std analyzed before sample analyses -95 -105% recovery limits p
Interference check solution analyzed at the beginning and the end of
the run (or every 8 hr-whichever is more frequent) with results p
within method required control limits of 80 -120%
Second source initial calibration verification and initial calibration
blank analyzed with results within method control limits p
CONTINUING CALIBRATION p
A continuing calibration verification standard (instrument check std)
and continuing calibration blank analyzed every IO samples and at p
the end of the analytical run with results within method control
limits
SAMPLE CRITERIA p
I. Analyzed within linear range of the curve
2. Serial Dilution (4X) performed if new matrix-(+/-) 10% of true p
I hereby certify that all the above information is correct to the best of my knowledge .. All out-of-control
measurements relating to the method required acceptance criteria have been documented in the above
table along with any known possible effects on the sample analytical data.
Name: Jaw.;.: S. Sol..wso,J
(print)
Name:~~
(sign)
QA Officer Signature: as.~ D.~
000082
Kubal-Furr & Associates
INSTRUMENT QC ASSESSMENT SUMMARY
FOR EPA METHOD 7470A/7471A
For Samples: lab ID #199011502-07 lab ID# lab ID#
lab ID #199011502-13 lab ID# lab ID#
lab ID# lab ID# lab ID#
lab ID# lab ID# lab ID#
lab ID# lab ID# lab ID#
lab ID# lab ID# lab ID#
CRITERIA P/F COMMENTS
INITIAL CALIBRATION:(a blank and at least 5 Date of calibration: 1 /20/99
standards with r 0.995 daily) p
All standards and solutions prepared/utilized within method
required holding times p
Second source initial calibration verification and initial
calibration blank analyzed immediately after calibration curve p
with results within method required control limits
CONTINUING CALIBRATION
A continuing calibration verification standard and continuing
calibration blank analyzed every IO samples and at the end of p
the analytical run with results within method required control
limits
SAMPLE CRITERIA
I. Analyzed within working range of the curve(<highest std) p
2. MSAs perfonned as needed and within method control p
limits
I hereby certify that all the above information is correct to the best of my knowledge. All out-of-
control measurements relating to the method required acceptance criteria have been documented
in the above table along with any known possible effects on the sample analytical data.
Name: DAN"' w . L.M
(print)
Name: tk .,,vJ. ~
(sign)
QA Officer Signature-M ~
Date: z t 11 / H j
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00008,1 ---•
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Kubal-Furr & Associates
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INSTRUMENT QC ASSESS.MENT SUMMARY
FOR EPA METHOD 8081A
For Samples: lab ID# L99011502-07 lab ID# lab ID# ----------
lab ID# L99011502-13 lab ID,# ____ _ lab ID# ____ _
lab ID# _____ lab ID# ____ _ lab ID# ____ _
lab ID# _____ lab ID# ____ _ lab ID# -----
CRITERIA P/F COMMENTS
INITIAL CALIBRATION:(at least 5 stds with one at Date of calibration: 1/5/98
or near MDL and use of dual column for confirmation) p
All standards and solutions prepared/utilized within method
required holding times p
External standard calculation used with r > 0.990 p
DDT and Endrin degradation < 15% p
DAILY OR CONTINUING CALIBRATION Date analyzed: 1/26/99
(beginning of each day and every 10 samples) p
Mid11oint calibration std run to verify: :,;ndrin recovered high (19%) in
I. Run midpoint cal std to check all analytes <15% Diff. F closing CCV (run 0126KA20). No
2. DDT and Endrin degradation< 15% p endrin was detected in the associated
3. I of2 Surrogate% rec within laboratory control limits p samples.
-SAMPLE CRITERIA
I. Bracketed by in-control CVs F See continuing calibration comment
2. I of2 Surrogates% rec within laboratory control limits p above.
3. Peak RT'window +/-3X Std. Dev. of the standard's RT p
4. Analyzed:within working range of the curve(<highest std) p
I hereby certify that all the above information is correct to the best of my knowledge. All out-of-
control measurements relating to the method required acceptance criteria have been documented
in the above table along with any known possible effects on the sample analytical data.
Name:_---'M....,.,,,c..,_h_,,c,e""-'\--'-A"" . ....,li-='-'-e:..•_,_oe,._,"-r __ _
(print)
Name: _ ___,_H....,i~W'.l"-'-",.., ~""'.)..,'-'--7;.,_,._,l.-l.A/lUA=""--'-'-°"'---
(sign)
QA Officer Signa
Date: z. ( I I / qq
000081
Kubal-Furr & Associates
INSTRUMENT QC ASSESSMENT SUMMARY
. FOR EPA METHOD 8151A
lab ID# L99011502-07 lab ID# lab ID# For Samples: -----

-
-
-
-
-
lab ID# L99011502-13 lab ID,# ____ _ lab ID# ____ _
lab ID# _____ lab ID# ____ _ lab ID# -----
lab ID# _____ lab ID# ____ _ lab ID# -----
CRITERIA P/F COMMENTS
INITIAL CALIBRA TION:(at least 5 stds with one at p Date of calibration: 11/13/98
or near MDL and use of dual column for confirmation)
External standard calculation used with r > 0.990 p
DAILY OR CONTINUING CALIBRATION p Date analyzed: 1/22/99,
(beginning of run and every 10 samples) 1/25/99
Midpoint calibration std run to verify:
I. Run midpoint cal std to check all analytes within 15% of p
true value
2. Surrogate% rec within lab generated control limits p
SAMPLE CRITERIA
I. Bracketed by in control CVs p Surrogate recovered low upon initial
2. Surrogate % rec within lab generated control limits p analysis. Re-injection passed. See case
3. Analyzed within working range of the curve(<highest std) p narrative.
I hereby certify that all the above information is correct to the best of my knowledge. All out-of-
control measurements relating to the method required acceptance criteria have been documented
in the above table along with any known possible effects on the sample analytical data.
Date: ;;../11 /99 '
Name: _ __,_H~ic.,_}:p---""',...,Q_..Au.c.-...J.)_...,,~"""'=-,,___ __ _
(sign)
000085
Kubal-Furr & Associates
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' INSTRUMENT QC ASSESSMENT SUMMARY
FOR EPA METHOD 8260B
For Samples: lab ID #L99011502-07 lab ID# ____ _ lab ID# ------
lab ID #L99011502-13 lab ID# ____ _ lab ID# ____ _
lab ID# _____ lab ID# ____ _ lab ID# ------
lab ID# _____ lab ID# ____ _ lab ID# ------
CRITERIA P/F COMMENTS
INITIAL CALIBRATION :(at leasts stds with one at p Date of calibration: 1 /19/99
or near MDL) -
All standards and solutions prepared/utilized within method p
required holding times
BFB Tune Criteria(table 3) p Time(s) of tuning: 06:51
SPCCs-criteria met in section 7.4.3.1 in method 8260A p
¾RSD for all analytes < 15%(use avg. relative RF for calc. or p
calculate cal curve with r ;:,o.990)
¾RSD for all analytes >15%(calculate cal curve with r p
;:,0.990)
CCCs ave RFs ¾RSD < 30 p
DAILY OR CONTINUING CALIBRATION p Date analyzed: 1/20/99
(beginning <if.each day and every 12 hr)
BFB Turie Criteria(table 3) p Time(s) of tuning: 07:48
Midpoint calibration std run to verify:
I. SPCCs -criteria met in section 7.4.3.1 in method 8260A p
2. CCCs %Drift < 20 p
3. Internal Standards RT within 30 sec of last check std(or cal) p
4. ElCP area for ISs -50% to + 100% from last check( or cal)
p
SAMPLE CRITERIA
1. Run within 12hr of last in-control tune p
2. Surrogate % rec within laboratory control limits p
3. TICs -ions> 10% of most abundant ion and NA TICs not required.
relative intensities of major ions agree within 20% p
4. Analyzed within working range of the curve(<highest std)
I hereby certify that all the above mfonnation 1s correct to the best of my knowledge. All out-of-control
measurements relating to the method required acceptance criteria have been documented in the above
table along with any known possible effects on the sample analytical data.
Name: Yo,,t.Jo.. A. {).,JI '½j Date: .:!· 11 ~~ C,
(print)
Name: (}°4~gt· ~
QA Officer Signatur L .D .. _J'(\--'.__,_...,,_
00008G
'
A..l'llll..J'A.A.'-V.1.•£,,_,,.,,_ "<._.,,.._...,,_._...,, .. , ___ ,_ ---·-·-----
FOR EPA METHOD 8270C
'
For Samples: Jab ID #199011502-07
lab ID #199011502-13
Jab ID#
Jab ID# ____ _
Jab ID# __ --'-----
lab ID# ------------
CRITERIA P/F
'
INITIAL CALIBRA TION:(at least 5 stds with one at or near MDL) p
All standards and solutions prepared/utilized within method holding p
times
DFTPP Tune Criteria(table 3) p
DDT degradation< 20% (applicable if determining pesticides) NA
Benzidine and/or pentachlorophenol present ai normal responses with p
no peak tailing visible(chromatography check std)
Components of interest with RTs of0.80 -1.20 relative to one of the p
Internal Standards
SPCCs -minimum avg. RFs = 0.05 p
%RSD for all analytes < I 5%(use avg. relative RF for calc. or calculate p
cal curve with r <! 0.990)
%RSD for all analytes > I 5%(calculate cal curve with r <! 0.990) F
CCCs ave RFs %RSD < 30% p
DAILY OR CONTINUING CALIBRATION p
(beginning of each day and every 12 hr)
DFTPP Tune Criteria(table 3) p
MidQoint calibration std run to veritv:
I. SPCCs -minimum avg. RFs = 0.05 p
2. CCCs %Drift in concentration < 20% p
3. Internal Standards RT within 30 sec of last check std(or cal) p
4. EICP area for !Ss -50% to + I 00% from last check( or cal) p
SAMPLE CRITERIA
I. Run within I2hr of last in-control tune p
2. Surrogate % rec within laboratory control limits p
3. TICs -ions> IO% of most abundant ion and NA
relative intensities of major ions agree within 20%
4. Analyzed within working range of the curve(<highest std) p
lab ID# ------lab ID# ____ _
lab ID# ------
COMMENTS
Date of calibration: 1/22/99
Time(s) of tuning: 09:28
Pesticides analyzed by 808 IA.
Pentaclorophenol r = 0.962
Date analyzed: 1/25/99
Time(s) of tuning: 08:11
'
TI Cs not required.
I hereby certify that all the above mformatlon 1s correct to the best of my knowledge. All out-of-control
measurements relating to the method required acceptance criteria have been documented in the above table along
with any known possible effects on the sample analytical data.
Name: Prw h & . .{),.J/'4-j Date: ;z.-/)--<f'-1
(print)
Name: P~n1 /)~
QA Officer Signatur<:J"-l DjW
000087
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Paralll•ter
Trace Metal ■ TCLP
SW846 1311
ARSENIC, TOTAL
BARIUM, TOTAL
CADMIUM, TOTAL
CHROMIUM, TOTAL
LEAD, TOTAL
SELENIUM, TOTAL
SILVER, TOTAL
Prep Procedure
Method Blanks
Blank MB15906:1
Method
Analytical Prep Procedure■:
METALS PREP ICP SWB46 3010
Cone
< 0.050
< 0.020
< o.ooso
< 0.010
< 0. 050
< 0,050
< 0.010
Analy■

t

Prep Date
Report Date
Page 1 of 1
: January 28, 1999
Matrix Leachate
WorkGroup: WG15906
Qual RDL Unit■ Analy ■t Date
0.050 mg/1 JSJ 01/19/99
0.020 mg/1 JSJ 01/19/99
0.0050 mg/1 JSJ 01/19/99
0.010 mg/1 JSJ 01/19/99
0.050 mg/1 JSJ 01/19/99
0.050 mg/1 JSJ 01/19/99
0.010 mg/1 JSJ 01/19/99
JSJ 01/19/99 1030
000088
Time
1613
1613
1613
1613
1613
1613
1613
Davis & Floyd, Inc. I PO Drawer 428 1 Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 l [phone] I Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Para.m•t•r
Trace Metals TCLP
SWB46 1311
ARSENIC, TOTAL
BARIUM, TOTAL
CADMIUM, TOTAL
CHROMIUM, TOTAL
LEAD, TOTAL
SELENIUM, TOTAL
SILVER, TOTAL
Prep Procedure
Method Blanks
Blank : EB15906:1
Method
Analytical Prep Procedures:
METALS PREP ICP SW846 3010
Cone
< 0. 050
< 0.020
< 0.0050
< 0. 010
< 0.050
< 0.050
< 0.010
Analyst Prep Date
Report Date
Page 1 of 1
: January 28, 1999
Matrix Leachate
WorkGroup: WG15906
Qual ROL
o.oso mg/1 JSJ
0. 020 mg/1 JSJ
0.0050 mg/1 JSJ
0.010 mg/1 JSJ
0.050 mg/1 JSJ
0. 050 mg/1 JSJ
0. 010 mg/1 JSJ
JSJ 01/19/99 1030
ooooan
Time
01/19/99 1718
01/19/99 1718
01/19/99 1718
01/19/99 1718
01/19/99 1718
01/19/99 1718
01/19/99 1718
Davis & Floyd, Inc. I PO Drawer 428 1 Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 l [phone] I Fax [phone]
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DL\VIS
FLOYD LABORATORY ANALYSIS REPORT
Param•t•r
Trace Metals TCLP
SWB46 1311
ARSENIC, TOTAL
BARIUM, TOTAL
CADM rm~, TOTAL
CHROMIUM, TOTAL
LEAD, TOTAL
SELENIUM, TOTAL
SILVER, TOTAL
Prep Procedure
Method Blanks
Blank : EB15906:2
Method
Analytical Prep Procedures:
METALS PREP ICP SWB46 3010
Cone
' 0 .oso
' 0. 020
' o.ooso
' 0.010
' o.oso
' 0. 050
' 0. 010
Analyst Prep Date
Report Date
Page 1 of
January 2s, 1999
Matrix Leachate
WorkGroup: WG15906
Qual RDL Units Analyat Date
0 .050 mg/1 JSJ Ol/19/9<J
0 .020 mg/1 JSJ 01/19/99
0.0050 mg/1 JSJ Ol/19/99
0.010 mg/1 JSJ 01/19/99
0.050 mg/1 JSJ Ol/19/99
o.oso mg/1 JSJ 01/19/';;9
0. 010 mg/1 JSJ 01/19/99
JSJ 01/19/99 1030
000090
Time
1722
1722
1722
1722
1722
1722
1722
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I {864) 229-4413 I Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS : LCS15906:l
ARSENIC, TOTAL 2.00
BARIUM, TOTAL 40.00
CADMIUM, TOTAL 0. 400
CHROMIUM, TOTAL 2.00
LEAD, TOTAL 2.00
SELENIUM, TOTAL 0.400
SILVER, TOTAL 2.00
1.93
35. 00
0. 368
1. 86
1.76
0. 375
1. 78
Report Date : January 28, 1999
Page 1 of 1
Matrix Leachate
WorkGroup: WG15906
Method SW846 1311
96. 5 80-120
87.5 80-120
91.9 80-120
93 .0 80-120
88.0 80-120
93.8 80-120
89.0 80-120
000091
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue l Greenwood, SC 29649 I {864) 229-4413 I Fax [phone]
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Di\YIS
FLOYD LABORATORY ANALYSIS REPORT
:/:-\;·~ra~"et~r
ARSENIC, TOTAL
BARIUM, TOTAL
CADMIUM, TOTAL
CHROMIUM, TOTAL
LEAD, TOTAL
SELENIUM, TOTAL
SILVER, TOTAL
· :.: Parani_eter
ARSENIC, TOTAL
BARIUM, TOTAL
CADMIUM, TOTAL
CHROMIUM, TOTAL
LEAD, TOTAL
SELENIUM, TOTAL
SILVER, TOTAL
Matrix Spikes and Duplicates
MS/MSD MS99011502-13:15906
MSD99011502-13:15906
1.00
20. 00
0. 2 00
1.00
1..00
0 . 200
1.00
1.00
20. 00
0 . 200
1 . 00
.oo
0. 200
l.00
< 0.0500
4. 48
< 0.00500
< 0.0100
< 0.0500
0.0840
< 0.0100
0. 948
21. 40
0 -181
0.895
0. 843
0. 290
0. 876
Report Date
Page 1 of l
January 28, 1999
Matrix Leachate
WorkGroup: WG15906
Method SW846 1311
o. 951 95 .1
21. 60 85. 6
0.184 91 . 9
0.899 89 .9
0 .848 84.8
0.288 102.0
0. 880 88.0
94.8 0.316
84.6 0.930
90.3 1. 76
89.5 0.446
84. .3 0.591
103.0 o. 692
87.6 0.456
000082
Li"mits':
:-~R~C. ::, ..
50-150
50-150
50-150
50-150
50-150
S0-150
50-150
20
20
20
20
20
20
20
50-150
50-150
50-150
50-150
50-150
50-150
50-150
Davis & Floyd, Inc. l PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue 1 Greenwood, SC 29649 1 [phone] I Fax [phone]
Di\YIS
FLOYD LABORATORY ANALYSIS REPORT
Parameter
Trace Metals TCLP
SW846 1311
MERCURY, TOTAL
Prep Procedure
Method Blanks
Blank : MB159-43: 1
Method
Analytical Prep Proceduree:
SW846 7470A
Report Date : January 2B, 1999
Page 1 of 1
Matrix Leachate
WorkGroup: WG15943
Cone Qual RDL Unite Analyst Date Tiine
< 0.00020 0.00020 mg/1 BDL 01/21/99 1214
Analyet Prep Data
BDL 01/20/99 1200
OOOOD;J
Davis & Floyd, Inc. I PO Drawer 428 1 ·creenwood, SC 29648 I 816 E. Durst Avenue ] Greenwood, SC 29649 I [phone] I Fax [phone]
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Parameter
Trace Metals TCLP
SW846 1311
MERCURY, TOTAL
Prep Procedure
Method Blanks
Blank : E:815943:1
Method
Analytical Prep Procedures:
SW846 7470A
<
Report Date
Page 1 of l
January 28, 1999
Matrix Leachate
WorkGroup: WG15943
Cone Qual RDL Onita Analyat Date
0.00020 0.00020 mg/1 BDL 01/21/99 1225
Analyat Prep Data
BDL 01/20/99 1200
000091
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS LCSl.5943: 1
MERCURY, TOTAL
Report Date : January 28, 1999
Page 1 of 1
Matrix : Leachate
WorkGroup: WG15943
Method : SWB46 1311
0.00200 0.00199 99.5 88-112
000095
Davis & Floyd, Inc. l PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] j Fax [phone]
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
:·: \';'=>"-.: . )·' -.:""
_Paiame.te!r
MERCURY, TOTAL
. '-~l:~~m~~~~ ·
MERCURY, TOTAL
MS/MSD MS99011502-13:15943
MSD99011502-13:15943
. 'Spi·ke: Sa_mple. ';_d~:;•t: .·_,-.'.<cane.
Report Date
Page 1 of 1
Matrix
January 28, 1999
Leachate
WorkGroup: WG15943
Method SW846 1311
0.00100 < 0.000200 0.000946 94.6
· .. ··.· Limitn
. ::\REC
50-150
spike. ·.:-: MSD
. Add~d-_;-.:. ··::_Cone.
0.00100 0.000880
· Mso ·:
··.:: \REC
88.0
·--./
·::,;:.\R·Po ·
7.23
000098
Limit:,
\RPO \REC
20 50-150
I Davis & Floyd, lnc. I PO Drawer 428 I Greenwood, SC 29648 1 816 E. Durst Avenue ] Greenwood, SC 29649 l [phone] I Fax [phone]
DAYIS
FLOYD
Method Blanks
Blank : MB16002:1
Paaticidaa and Herbicides TCLP
SW846 1311/BOBlA
CHLORDANE, TECHNICAL
ENDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
LINDANB
METHOXYCHLOR
TOXAPHENE
Analytical Prep Procedures:
Method
LABORATORY ANALYSIS REPORT
Cone
< 5.0
< 1. 0
< 0 . so
< 0 .so
< 0.50
< 5.0
< 50.0
Analyat Prep Date
Report Date
Page 1 of 1
Matrix
: January 28, 1999
Leachate
WorkGroup: WG16002
Qual RDL Unit• Analy■t Date
5.0 ug/1 KLH 01/26/99
1.0 ug/1 KLH 01/26/9YJ
0 .so ug/1 KLH 01/26/99
0. so ug/1 KLH 01/26/99
0 . so ug/1 KLH 01/26/99
5.0 ug/1 KLH 01/26/99
so.a ug/1 KLH 01/26/99
Time
1614
1614
1614
1614
1614
1614
1614
TCLP PESTICIDES SWB46 1311/3510C JMT 01/26/99 0730
000097
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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FLffi'D LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS
:.:-,.:.:::::•;_i·:::._ .. :_:.\'/::·:_·.
· ,/._P_.i~a_nie_ t:,:er
ENDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
LINDANE
METHOXYCHLOR
: LCS16002:1
: ::\A~Pd_. 0di~e./d>\?( :;::._i_:~~~-
. __ ___ -(~6-nC.
5.00 4.72
2.00 1.46
5.00 3.59
2.00 1.60
20.00 19.52
Report Date
Page 1 of 1
January 28, 1999
Matrix Leachate
WorkGroup: WG16002
Method SW846 1311/SOBlA
.. ,.:·:.:"'iCS\: ·· : .. :, ·-···:-:-c::,:·Li~i-t·~\(./:": ·
. : ·.::/{\;Ji/<<····· \"RE.~-.
H.4
73 .0
71. 9
80.1
97. 6
70-130
70-130
70-130
70-130
70-130
000098
Davis & Floyd, lnc. I PO Drawer 428 ! Greenwood, SC 29648 1 816 E. Durst Avenue I Greenwood, SC 29~49 I {864) 229-4413 I Fax [phone]
D1\VIS
FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
ENDRIN
HEPTACHLOR
HBPTACHLOR EPOXIDB
LINDANB
MSTHOXYCHLOR
ENDRIN
HEPTACHLOR
HBPTACHLOR EPOXIDE
LINDANB
MBTHOXYCHLOR
MS99011502-07:16002
MSD99O115O2-O7:16O02
5.00
2.00
5.00
2.00
20.00
5.00
2.00
5.00
2.00
20. 00
< 1.00
< o.soo
< 0.500
< 0.500
< 5.00
4. 77
1. 57
3.68
1.65
17. 93
Report Date
Page 1 of 1
: January 28, 1999
Matrix Leachate
WorkGroup: WG16002
Method SW846 1311/BOSlA
4.91
1. 58
3.82
1.65
19. 78
95,5
78 .5
73. 5
82.5
89.6
98.2
79.2
76.S
82.6
98.9
2,78
0.913
3,93
0. 218
9.82
oooosn
50-108
30-103
51-94
39-101
61-110
20
20
20
20
20
50-108
3 0-103
51-94
39-101
61-110
Davis & Floyd, Inc. I PO Drawer 428 I Creerlwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] \ Fax [phone]
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
'°:'.}tZ:::~~~r-·
ENDRIN
HBPTACHLOR
HSPTACHLOR BPOXIDB
LINDANB
METHOXYCHLOR
BNDRIN
HBPTACHLOR
HBPTACHLOR BPOXIDB
LINDANE
MBTI-lOXYCHLOR
Report Date
Page 1 of 1
: January 28, 1999
Matrix Leachate
MS99011502-13:16002
MSD99011502-13:16002
WorkGroup: WG16002
Method SWB46 1311/BOBlA
· Spikei•:··:-·::···. ;:/ Sanipi-~·/'. :·. MS··, ·: ·::_ MS.\·-:
-'~aded ·/> ·-:·::c~n/"': c~~/ .. _. .,.:· ~REC\'".
5.00
2.00
.00
2.00
< 1.00
< 0.500
< 0.500
< 0.500
5.01
1. 64
3.87
1. 72
20.00 < 5.00 20.37
Sp.ik~··::. MSD : "MSD
~~~;d\//\(\:o·n~='/ .-· ::._\is~-;
5.00
2.00
5.00
2.00
20.00
5.09
. 74
3.91
1. 74
20. 46
101.7
87.0
7EL 1
87.1
102 .3
100.2
82.1
77. 5
86.0
101.8
1.51
5. 84
0.887
1.26
0. 445
000100
· Limits. ~;-~c .-:
50-108
30-103
51-94
39-101
61-110
Litllito·· : <\~-PD: .. :\~Ee.
20
20
20
20
20
50-108
30-103
51-94
39-101
61-110
Davis & Floyd, Inc. I PO Drawer 428 I Greenvvood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLtJ\'D LABORATORY ANALYSIS REPORT
Surrogates % Recovery
L99011502-07
L99011502-l3
LCS16002:1
MB16002:l
MS99D11502-07:16002
MS99011502-13:16002
MSD99011502-07:16002
MSD99011502-13:16002
DCB DBCACHµ,ROBIPHBNYL
TCX TSTRACHLORO-M-XYLENE
MeasureDate
26-JAN-99 18:09
26-JAN-99 20:04
26-JAN-99 16:52
26-JAN-99 16:14
26-JAN-99 18:48
26-JAN-99 20: 42
26-JAN-99 19:26
26-JAN-99 21: 20
74.0
86.5
82.0
78.9
7 5. 1
85.9
77.3
88.4
Report Date
Page 1 of l
January 28, 1999
Matrix GW/ChemW
Method SW846 1311/8080
67.5
72 .o
63.6
63.4
64.9
68.5
68.4
74.3
000101
Davis & Floyd, Inc. I PO Drawer 428 j Greenwood, SC 29648 I 816 E. Ours! Avenue [ Greenwood, SC 29649 \ [phone] I Fax [phone]
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FLOYD
Method Blanks
Blank MB15935: 1
Parameter
Peaticidea and Herbicide ■ TCLP
SWB46 l3ll/8151A
2,4,5-TP (SILVEX)
2,4-D
Prep Procedure
Analytical Prep Procedures:
Method
LABORATORY ANALYSIS REPORT
<
<
Cone
0.10
1.0
Analyst Prep Date
Report Date
Page l of 1
January 28, 1999
Matrix Leachate
WorkGroup: WG1593S
Qual RDL
0.10
1.0
Onita Analyat Date Tim•
ug/1
ug/1
KLH 01/22/99 1817
KLH 01/22/99 1817
TCLP HERBICIDES SW846 1311/BlSlA JMT 01/20/99 1500
000102
Davis & Floyd, Inc. I PO Drawer 428 l Greenwood, SC 29648 l 816 E. Durst Avenue j Greenwood, SC 29649 I [phone] I Fax [phone]
Df\YIS
FLOYD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS
t:'.(}[i!l'.:_j_-~ti_:;:: ._,.. ;
2·,4,5-TP {SILVEX)
2,4-D
LCS15935:1
Report Date
Page 1 of 1
Matrix
January 28, 1999
Leachate
WorkGroup: WG1S935
Method SW846 1311/BlSlA
. .,.._.·,:.•sp•iki: ':'··::::.:::-:::::r.;"c"s··::·:-... --· :,::::.1,c,s:::=:::" ,: ·\:·,_::'}Lirii:I't~:::>,:-•:• ,.
···:14~';Jil: V\';:::::;:;:~~tJ::::; :::\/:)f'.J.~il:::/ :;::::;::/\::::;:J,~~·-::':::_:_::,··:;'\··.
5.00
50. 00
3.93
41.51
78.6
83.0
70-130
70-130
000103
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst' Avenue I Greenwood, SC 29649 I [phone] 1 Fax [phone]
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FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
f();~~~~~~;
2,4,5-TP (SILVEX)
2,4-D
.):":_) .. -:•:·:. .
\/~~-~amet.~r
2,4,5-TP (SILVEX)
2,4-D
Report Date
Page 1 of 1
January 28, 1999
Matrix Leachate
MS99011502-07:l5935
MSD99011502-07:l5935
WorkGroup: WG15935
Method SW846 1311/BlSlA
·s·· ·.·~---' ·:.:::,·:::,: iI~~Pi~ · ,-:_·.M-s:/,','0··· ,·Ms.
A
. pd•d~.·.•.:·•·•d~:: ... :.. . . . . -

·

.. ·.·-.-.. -.... . . ....... -p:.\:/ .. C~h{)) -:-'.<>(t~?h/// .-·,:.-:.:::.::_:i~EC-
5 .00 < 1.00 4.69 93.9
so.co < 10.00 45.81 91.6
5.00
so.co
3. 96
38.69
79.2
77.4
00010'1
16.9
16,8
·-:::..,: Li.mi tO
-,~·Ee· ..
42-131
39-147
· · ·Limito
\RPD \REC· .. .--
20 42-131
20 39-147
I Davis & Floyd, Inc. I PO Drawer 428 \ Greenwood, SC 29648 \ 816 E. Durst Avenue \ Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLt1YD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
\\'b_~::lmet'~;:. -·
2,4,S·TP (SILVEX)
2,4-D
p'~~~~~.t·~·r.
2,4,5-TP (SILVEX)
2, 4 ·D
Report Date
Page 1 of 1
: January 29, 1999
Matrix Leachate
WorkGroup: WG15935 MS99011502-13:15935
MSD99011502-13:15935 Method SW846 1311/8151A
: :_:·As. pd'i.id:'.:•k,:}d•J .. '..';:·.'.:,::,'..:,·:,·. . Sa_~Pl_e: .. · .. , .. M.t ..... '.:'." ....... :· .. :'..:/.:.Mf .. _____ . ::\ :. ·col'1C{·.·:·· :·t(d~rict :/:(_./::(~Rfc·:-·.
s.oo o.oo 4.21 84.0
so.oo 0.00 40. 88
.. Spi'~~\>
--A~~~~\
5.00
so. 00
4.28
46.53
86.0
93.0
000105
81.0
2.40
13 .8
.i.i~/to},.··i·
\RE'c•·
42-131
39-147
Liin,i°to . · .
. \R~~ \R_EC
20
20
42-131
39-147
Davis & Floyd, Inc. \ PO Drawer 428 I Greenwood, SC 29648 1 816 E. Durst Avenue \ Greenwood, SC 29649 I (864) 229•4413 I Fax [phone]
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Surrogates % Recovery
SampleJ:1um MeasureDate
L99011502-D7 22-JAN-99 19:28
L99011502-13 25-JAN-99 13:25
LCS15935:1 22-JAN-99 18: 41
MB15935:1 22-JAN-99 18:17
MS990ll502-07: 15935 22-JAN-99 19: 51
MS99011502-13: 15935 22-JAN-99 21; 01
MSD99011502-07:15935 22-JAN-99 20: 15
MSD99011502-13:15935 22-JAN-99 21 : 25
OTHER -2,4-DICHLOROPHENYLACETIC ACID
OTHER"
· 70:.~.:2·7.
78,8
76.4
88.8
92.0
99.5
87.0
86.5
93.0
Report Date
Page 1 of
Matrix
Method
00010G
January 28, 1999
GW/ChemW
SWB46 1311/8150
Davis & Floyd, Inc. 1 PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Method Blanks
Blank
Param•t•r
Volatile Organics TCLP
SW846 13ll/B260B
1,1-DICHLOROETHENE
1,2-0ICHLOROETHANE
2-BUTANONE
BENZENE:
CARBON TETRACHLORIDE
CHLOROBENZENB
CHLOROFORM
TETRACHLOROETHENE
TRICHLOROETHENE
VINYL CHLORIDE
Prep Procedure
Analytical Prep Procedures:
ZHE EXTRACTION
MB15885:l
Method
SWB46 1311
Report Date
Page 1 of 1
Matrix
January 2B, 1999
Leachate
WorkGroup: WG15885
Cone RDL Units Analyst Date
' 5.0 5.0 ug/1 PAP 01/20/99
' 5.0 5 .0 ug/1 PAP 01/20/99
' 10.0 10.0 ug/1 PAP 01/20 /99
' 5.0 5. 0 ug/1 PAP 01/20/99
< 5.0 5 .0 ug/1 PAP 01/20/99
' 5.0 5 .0 ug/1 PAP 01/20/99
' 5.0 5.0 ug/1 PAP 01/20/99
' 5.0 5. 0 ug/1 PAP 01/20/99
' 5.0 5. 0 ug/1 PAP 01/20/99
' 10.0 10.0 ug/1 PAP 01/20/99
Analyst Prep Date
DBC 01/18/99 1500
00010'7
Tillle
0925
0925
0925
0925
0925
0925
0925
0925
0925
0925
Davis & Floyd, Inc. I PO Drawer 428 1 Greenwood, SC 29648 ] 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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FLOYD
Method Blanks
Blank
Param•t•r
Volatile Organics TCLP
SW846 1311/8260B
1,1-DICHLOROETHENE
1,2-DICHLOROBTHANB
2-BUTANONE
BENZENE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROFORM
TBTRACHLOROETHENE
TRICHLOROETHENE
VINYL CHLORIDE
MB15899:l
LABORATORY ANALYSIS REPORT
<
<
<
<
<
<
<
<
<
<
Cone
5.0
5.0
10.0
5.0
5.0
5.0
5.0
5.0
5.0
10.0
Report Date
Page 1 of l
January 28, 1999
Matrix Leachate
WorkGroup: WG15899
Qual RDL Onita Analyst Oat•
5.0 ug/1 PAP 01/20/99
5.0 ug/1 PAP 01/20/99
10.0 ug/1 PAP 01/20/99
5.0 ug/1 PAP 01/20/99
5. 0 ug/1 PAP 01/20/99
5.0 ug/1 PAP 01/20/99
5.0 ug/1 PAP 01/20/99
5.0 ug/1 PAP 01/20/99
5.0 ug/1 PAP 01/20/99
10.0 ug/1 PAP 01/20/99
000108
0904
0904
0904
0904
0904
0904
0904
0904
0904
0904
Davis & Floyd, Inc. I PO Drawer 428 I Cre('nwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I {864) 229-4413 I Fax [phone]
D~IS
FLOYD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS
:::::1:;::;~:j~~~ti;-:
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
2-BlITANONE
BSNZSNE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROFORM
TETRACHLOROETHENE
TRICHLOROETHENE
VINYL CHLORIDE
: LC'Sl5885:1
Report Date
Page 1 of
Matrix
: January 28, 1999
Leachate
WorkGroup: WG15885
Method SW846 1311/8260B
. ·-\-\-.·:://:~'P{i2~'fj ·,:::::=:::Les·>=·==·:. :.·::::·:=:test}'::=.
·=-·'-:.:\.·.:tA~d~J?:t ·i::::\{~.o~/J: ?/:():\~121(\::": <·)\\~-~:~-,
20.00 14.76 73, B 61-128
20.00 23.31 116.6 77-140
20.00 22.97 11-4 .9 31-161
20.00 20.03 100.2 77-127
20.00 17.37 86.9 63 -13 3
20. 00 21. 98 109.9 87-124
20.00 23 . 4 6 117 .3 83-131
20. 00 17.97 89. 9 73-129
20 . 00 20 .01 100.1 77-130
20 .00 13 .34 66.7 45-162
00010n
Davis & Floyd, lnc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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FLOYD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS
i//p·~;~meter_· ·
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
2-BUTANONE
BENZENE
CARBON TETRACHLORIDE
CHLOROBENZENB
CHLOROFORM
TETRACHLOROETHENE
TRICHLOROETHENE
VINYL CHLORIDE
LCS15899:l
· ... _S_p_i_k:~//1-··· ·'Lc·s::-:-·
·. 'Ad'3:e.d . '.:/~~·n'~·-:·
20.00 15. 02
20.00 22.65
20. 00 25. 32
20. 00 19.85
20 . 00 17. 30
20 00 22.36
20. 00 23.07
20. 00 18. 24
20 .00 19.n
20. 00 12.82
Report Date
Page 1 of 1
: January 2B, 1999
Matrix Leachate
WorkGroup: WG15899
Method SW846 1311/8260B
: .. CLCs::.
\REC_·_.·
75.1
113. 3
12 6. 6
99.3
86.5
111. B
115 .4
91.2
99.6
64.1
·-··L{mit~ \/\i·sc·,.:-··
61-128
77-14.0
31-161
77-127
63-133
87-124
83-131
73-12 9
77-130
45-162
00011.0
Davis & Floyd, Inc. 1 PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax {864) 229-7119
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSO
,_.:-.. :-:.-::.-. ..
':.y,p~;:am~-~er
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
2-BUTANONE
BENZENE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROFORM
TETRACHLOROETHENE
TRICHLOROETHENE
VINYL CHLORIDE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
2-BUTANONE
BENZENE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROFORM
TETRACHLOROETHENE
TRICHLOROETHENE
VINYL CHLORIDE
MS99011502-07:15899
MSD99011502-07:15899
Report Date
Page 1 of 1
Matrix
: January 20, 1999
Leachate
WorkGroup: WG15899
Method SWB46 1311/82608
:·sP~f§.:{\+ .:.::::tS~ciPi~t \:G/Ml.::-:.
Adae:a·::· ·· :\f;:rii:( .. ..-,::,:::\::\Cci~~
·,.t=Ms<-: :,>({;;I)···,·· Li~ii·t·~t/·i-=:··. ·.\-~i~::,•
500.0 < 50. 00 434.8
500.0 < so.oo 550. 3
500. 0 < 100.0 563.8
500.0 < 50. 00 475. 4
500.0 < 50.00 507.1
500.0 ' so. 00 517.9
500.0 ' 50. 00 563.1
500.0 ' 50.00 463.6
500.0 ' 50.00 498.l
500. 0 ' 100. 0 355. 6
500.0 441.7 88.3
500.0 574.0 114. 8
500.0 614 .1 122.8
500.0 481.7 96.3
500.0 523. 3 104 .7
500.0 520.5 104. 1
500.0 581. 2 116 • 2
500.0 472 .4 94.5
500.0 503.2 100.6
500.0 382. 7 76.5
000111
87.0
110 .1
112 .B
95.1
101.4
103.6
112. 6
92.7
99.6
71.1
1. 58
4. 22
8.55
1. 32
3.15
0.493
3.17
l. 88
1.01
7.34
67-126
75-132
65-142
77-119
74-131
85-117
82-127
71-129
80-124
51-157
13
15
33
13
14
13
12
14
14
25
67-126
75-132
65-142
77-119
74-131
85-117
82-1.:17
71-129
80-124
51-157.
Davis & Fiord, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue 1 Greenwood, SC 29649 l [phone] I Fax {864) 229-7119
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FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSO
i,:·:\;~*a~:~·t~r
1,1-DICHLOROETHENE
1,2-DICHLOROETH!,.NE
2-BUTAN'ONE
BENZENE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROFORM
TETRACHLOROETHENE
TRICHLOROETHENE
VINYL CHLORIDE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
2-BUTANONE
BENZENE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROFORM
TETRACHLOROETHENE
TRICHLOROETHENE
VINYL CHLORIDE
MS99011502-13:15885
MSD99011502-13:15885
·•-i;i·~~:·(// ·c:•s~_mpi,;-.:-:
11.a_de?,::-·co;.;c·.::·:
500.0 < SO.OD
soo.o < so.co
500.0 < 100. 0
soo. 0 < 50.00
500.0 < SO.OD
500.0 < SO.DO
500 .0 < 50.00
500. 0 < 50. 00
soo. 0 < SO.DO
soo.o < 100.0
500.0 473.B
500.0 586. 0
soo.o 702.8
500.0 494.9
500.0 565.6
500.0 526.9
500.0 596.6
500.0 485.9
500.0 515.5
500.0 388.4
Report Date
Page 1 of 1
January 28, 1999
Matrix Leachate
WorkGroup: WG15885
Method SW846 1311/8:HOB
MS
cone
432.8
533.9
631. l
470. 0
524. B
505.B
546.B
476.6
495. 2
368.0
94.8
117 .2
140.6
99.0
113 .1
105. 4
119 .3
97 .2
103 .1
77. 7
;,\REC
86.6
106.8
12 6. 2
94.0
105. O
101.2
109. 4
95.3
99.0
73 .6
. : \RPD
9.05
9. 29
10.7
5.15
7.47
4.10
8. 71
1.94
4.03
5.40
Limito
\REC
67-126
75-132
65-142
77-119
74-131
85-117
82-127
71-129
80-124
51-157
Litrlit
\RPD ·
13
{R~~\:(:
15
33
13
14
13
12
14
14
25
67-126
75-132
65-142
77-119
74-131
85-117
82-12.7
71-129
B0-124
51-157.
000112
Davis & Floyd, lnc. I PO Drawer 428 I Greenwood, SC 29648 ! 816 E. Durst Avenue I Greenwood, SC 29649 I {864) 229-4413 [ Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Surrogates % Recovery
:'\SafupieNUm ·
L99011502-07
L99011502·13
LCS15885:l
MBlSBBS:1
MS99011207-0l:15885
MS99011502-13:15885
MSD99011207-0l:15885
MSD99011502-13:15885
LCS15899:l
MB15899:l
MS99011502-07:15899
MSD99011502-07:15899
··-MeasureDate
20-JAN-99 09:47
20-JAN-99 11:47
20-JAN-99 12:45
20-JAN-99 09:25
20-JAN-99 11:06
20-JAN-99 12:06
20-JAN-99 11:26
20-JAN-99 12:26
20-JAN-99 13:05
20-JAN-99 09: 04
20-JAN-99 10 :07
20-JAN-99 10: 26
DCB 1,2-DICHLOROETHANE·D4
BFB
TOL
BROMOFLUOROBENZENE
TOLUENE-DB
Report Date
Page 1 of 1
January 2B, 1999
Matrix GW/ChemW
Method
"'I'OL):'}t ··:·· . .-.,')\~/;}t:: /\?}ft)·. 83::.iii?'·
94.4 92. 5 101.s
99.0 92.S 99.9
105.6 96.4 98 .7
103.7 96.8 98. 0
104. ' 97.0 97.4
104 . ' 98.6 98.l
112 . 7 100.6 97.7
111.6 98 . 2 97.6
105.7 97. s 98.1
101. 9 91 .8 100.9
106 ., 98.0 96.3
111 . 7 98.6 96.9
000113
SW846 1311/8260
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 j 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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FLtwD
Method Blanks
Blank
Parameter
Semivolatile Organic• TCLP
SW846 13ll/8270C
1,4-DICHLOROBENZENB
2,4,S·TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DINITROTOLUENE
2-METHYLPHENOL
3&4-METHYLPHENOL
HEXACHLOROBENZENB
HBXACHLOROBUTADIENB
HBXACHLOROETHANE
NITROBBNZENE
PENTACHLOROPHENOL
PYRIDINE:
Prep Procedure
: MB15915:l
Method
Analytical Prep Procedures:
LABORATORY ANALYSIS REPORT
Cone
< 100
< 100
< 100
< 100
< 100
< 100
< 100
< 100
< 100
< 100
< 250
< 100
11.naly ■t Prep Date
Report Date
Page 1 of 1
; January 28, 1999
Matrix Leachate
WorkGroup: WG15915
Qual RDL
100 ug/1 DSD/JRN
100 ug/1 DSD/JRN
100 ug/1 DSD/JRN
100 ug/1 DSD/JRN
100 ug/1 DSD/JRN
100 ug/1 DSO/JRN
100 ug/1 DSD/JRN
100 ug/1 DSD/JRN
100 ug/1 DSD/JRN
100 ug/1 DSD/JRN
250 ug/1 DSD/JRN
100 ug/1 DSD/JRN
Tim•
01/25/99 1021
01/25/99 1021
01/25/99 1021
01/25/99 1021
01/25/99 1021
01/25/99 1021
01/25/99 1021
01/25/99 1021
01/25/99 1021
01/25/99 1021
01/25/99 1021
01/25/99 1021
TCLP SEMIVOLATILES SWB46 1311/3SOOA JMT 01/20/99 0830
00011'1
Davis & Floyd, Inc. I PO Drawer 428 l Greenwood, SC 29648 l 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS : LCS15915: 1
3&4-METHYLPHENOL 2000.
PYRIDINE 500.0
1,4-DICHLOROBENZENE 500.0
2,4,5-TRICHLOROPHENOL 1000.
2,4,6-TRICHLOROPHENOL 1000.
2,4-DINITROTOLUENE 500.0
2-METHYLPHENOL 1000.
HEXACHLOROBENZENE 500.0
HEXACHLOROBUTADIENE 500.0
HEXACHLOROETHANE 500.0
NITROBENZENE 500.0
PENTACHLOROPHENOL 1000.
104 6.
200.6
299 .9
723 .0
696.3
380. 7
614.0
422.2
275.9
267.9
368.0
942.6
Report Date
Page 1 of 1
: January 28, 1999
Matrix Leachate
WorkGroup: WG15915
Method SW846 1311/8270C
52.3 15-117
40-1 19-90
60.0 30-10B
72.3 44-111
69.6 32-109
76.1 52-116
61.4 33-123
84.4 63-119
55 .2 2 5-96
53.6 20-105
73.6 41-124
94.3 34-125
000115
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
... '' p·~ran,e;e·r. :-.
3&4-M6THYLPHENOL
PYRIDINE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DINITROTOLUENE
2-METHYLPHENOL
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROETHANE
NITROBENZENE
PENTACHLOROPHENOL
3&4-METHYLPHENOL
PYRIDINE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DINITROTOLUENE
2-METHYLPHENOL
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROETHANE
NITROBENZENE
PENTACHLOROPHENOL
MS99011502-07:15915
MSD99011502-07:15915
.. :--1:ttl} :: ·
2000.
soo.o
500.0
1000.
1000.
500.0
1000.
500.0
500.0
500.0
500.0
1000.
2000.
500.0
500. 0
1000.
1000.
500. 0
1000.
500.0
500.0
soo.o
500.0
1000.
Report Date
Page 1 of 1
Matrix
: Janu&ry 28, 1999
Leachate
WorkGroup: WG15915
Method SWB46 13ll/8270C
:_: s;~pi~ : .. :·-.::: C::. Ms .
. ::\:o·~-~-( .. ::\\ C.::;~~\ (:::·:I
· MS· {µ:~·?'• i.ifflil:.of
-::·\Rsc
18-112
11-90
24-110
19-1"35
55-125
27-128
33-121
57-119
4-124
22-98
32-125
22-136
< 100.0
< 100.0
< 100.0
< 100.0
< 100.0
< 100.0
< 100. 0
< 100. 0
< 100.0
< 100. 0
< 100. 0
< 250.0
980.0
211.4
279.5
803.1
684.3
404.7
552.2
456. 9
281.B
262. 1
332 , 9
764.9
957. 4
207 , 5
266. 0
802. 1
688.1
431.4
547.7
462.8
252.8
244.2
329. 6
1019.
49.0
42.3
55.9
80.3
68.4
80.9
55.2
91.4
56.4
52.4
66.6
76.5
47.9
41. 5
53.2
00.2
68.B
86.3
54.8
92.6
50.6
48. 8
65.9
101.9
2.33
1. 86
4.95
0.125
0.554
6. 39
0. 818
1. 28
10.a
7.07
0.996
28.5
00011G
23 18-112
42 11-90
44 24-110
52 19-135
16 55-125
26 27-128
22 33-121
36 57-119 ·
38 4-124
41 22-98
36 32-125
44 22-136
0Jvis & Floyd, Inc. I PO Drawer 428 ! Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
Dl\VIS,
FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
3&4-METHYLPHENOL
PYRIDINE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DINITROTOLUENE
2-METHYLPHENOL
HEXACHLOROBENZENE
HBXACHLOROBUTADIENE
HEXACHLOROETHANE
NITROBENZENE
PENTACHLOROPHENOL
3&4-METHYLPHBNOL
PYRIDINE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DINITROTOLUENE
2-METHYLPHENOL
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROETHANE
NITROBENZENE
PENTACHLOROPHENOL
MS99011502-13:15915
MSD99011502-13:1591S
2000.
500.0
500.0
1000.
1000.
500.0
1000.
500.0
500.0
500. 0
500. 0
1000.
2000.
500. 0
500.0
1000.
1000.
500.0
1000.
500.0
500. 0
500.0
500 .0
1000.
' 100. 0
' 100.0
' 100. 0
' 100, 0
' 100. 0
' 100.0
' 100.0
' 100.0
' 100.0
' 100.0
' 100.0
' 250.0
1022.
239.7
313. l
818.S
749.1
407.8
594.1
482.1
309.6
290. 3
370.2
885.9
Report Date
Page 1 of
January 28, 1999
Matrix Leachate
WorkGroup: WG15915
Method SW846 1311/B270C
993.2 49.7
217.1 43.4
289. 7 57.9
852.9 85.3
739 .3 73.9
425 .1 85.0
569. 0 56. 9
492.5 98.5
285.5 57.1
267 .3 53.S
356 .3 71. 3
993.0 99.3
51.1 2.84
47.9 9.89
62.6 7.76
81-9 4.12
74.9 1.32
81.6 4.15
59.4 4.32
96.4 2 .13
61. 9 8.10
58.1 8.25
74.0 3.83
88.6 11.4
000117
--~ini~ts
. ·:: \RE¢
18-112
11-90
24-110
19-135
55-125
27-128
33-121
57-119
4-124
22-98
32-125
22-136
23
42
44
52
16
26
22
36
38
41
36
44
18-112
11-90
24-110
19-135
55-125
27-128
33-121
57-119.
4-124
22-98
32-125
22-136
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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FL'1YD LABORATORY ANALYSIS REPORT
Surrogates % Recovery
· ... : SaillpleNum
L99011502-07
L99011502-13
LCS15915:l
MB1S915: 1
MS99011502-07:15915
MS99011502-13:15915
MSD99011502-D7:15915
MSD99011502-l3:15915
MeasureDate
25-JAN-99 12:11
25-JAN-99 14 :01
25-JAN-99 10 :58
25-JAN-99 10: 21
25-JAN-99 12 : 4B
25-JAN-99 14 : 39
25-JAN-99 13 : 24
2S-JAN-99 15: 16
TBP 2,4,6-TRIBROMOPHENOL
FBP 2-FLUOROBIPHENYL
2FP 2-FLUOROPHENOL
NBZ NITROBENZENE-D5
PHL PHENOL·D5
TPH TERPHENYL-D14
TBP FBP
52:..115 42-110
85.1 78.6
86.8 64.3
Bl. 6 69.5
67.7 52.9
90.4 63.8
93.6 71 . 7
86. 9 67 . a
87.7 73 . B
Report Date ' January 2 B, 1999
Page 1 of 1
Matrix GW/ChemW
Method SW846 1311/8270
. 2FP NBZ PHL TPH
12-84 39-104 21-53 61-1.21
42.0 73.0 28.0 91. 6
35 .3 59 .6 25.7 89.2
42.6 70 . 7 30. 7 74 .5
29.6 49 . 9 21 .0 74 .7
37.7 61 . ) 27.4 84 . B
40. 2 66.7 28.4 91 .0
37.5 62 .6 27.6 87.3
41. 9 68 .6 29.6 90.6
000118
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] 1 Fax [phone]
DL\VIS
FLOYD LABORATORY ANALYSIS REPORT
Other Documentation
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000119 I
Davis & Floyd, Inc. I PO Drawer 428 j Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone] I
-- -- -- -
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Chain of. Custody Form
FL D 816 East Durst Street, Greenwood, S.C. 29649 Phone [phone] Fax [phone]
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CW-GROUND WATER RC-RCRA SW-SURFACE WATER IM-IMPINGER SOLUTION F -FILTERS
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PROJ. NO. PROJECT NAME CONTAINERS (PARAMETERS ON BACK)
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--
LOGIN.REPORT (ln0l)
Jan 19 1999, 02:15 pm
Login Number: L99011501
Account: HNAHOL-SHE HNA HOLDINGS INC.
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I Project: 60885.00 GW S&A REPLACES 60603.00
'
r.9.9P+.1so+EP:l t•••m••Mf,s.·~.·I
lt;w/ChemW S VO/8260
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PH Remarks
REF 126-1 *l 1M
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GW/ChemW S VO/8260
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PH Remarks
REF 126-1 *1 ,4.Ul:
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·• ., .. r ....... ~ ... // .. : • .. •ii .~ . ii:emiirk';· .t. ········.;". :::::
GW/ChemW S VO/8260 REF 126-1 *1 d/J:
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PH Remarks
GW/ChemW S VO/8260
I p999:u~,s•o:1,so·tit ·•··•·••<Kf··:2.••8t•••·><···•
I GW/ChemW
GW/ChemW ...
S VO/8260
S WC/TOC
REF 126-1 *l 1J.ltt
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REF 126-1 *1
REF 121-1 *2
PH Remarks ±--
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PH Remarks
GW/ChemW S VO/8260 REF 126-1 *1 dlir _______ _
GW/ChemW S WC/TOC REF 121-1 *2 J
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Reviewed: ·. :~tiZ~.fZ~.],;
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Signature: ';rf!i)y;Wrl[:9:[;]
:olitt:
000121
GW/ChemW
GW/ChemW
·Gw/ChemW
GW/ChemW
LOGIN REPORT (ln0l)
Jan 19 1999, 02:16 pm
Login Number: L99011502
Account: HNAHOL-SHE HNA HOLDINGS INC.
Project: 60885.00 GW S&A REPLACES 60603.00
'
ff\\J;4f\JAN£9.9 ·••••l<>.••;J.:2.•••t112iJAN£99.t$ .• r:27.·7;rANf.99.t••
PH Remar)<.s
S VO/8260 REF 126-1 *l (V,A
./ iil4FJ'ANP99i•••10T42}:i4 1 JANE.9•.9i/$·•cu:27;+J11,NS9·9.
PH Remarks
S VO/8260 REF 126-1 *l l'lfA
+i••·•t t+45iJANf•·99.\1Qd4.4%+1iiJANS9.9?/S}\i2.7/.JAN£9.9f
S VO/8260
PH Remarks
REF 126-1 *l /YA
f ty ? t,tfJANE9 9F1:l!:"2:J!ffl4+•;rAN.b••9.9)fl=l}%••:279;rANF99l
PH Remarks
S VO/8260 REF 126-1 *l --1'A
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PH,,,...,,, Remarks ·.
GW/ChemW
GW/ChemW
S VO/8260
S WC/TOC
REF 126-1 *l /f./,
REF 121-1 *2 L
L99•ott5•02pp·6. f \J:ts:tC:t\ <•·••·>•••?•• ····•··•·•·•·•·•···•·•··•··•·•··••.••·•••·· t·•·t4p.rAN+•99t:Lli(4+II:i."4Sti:ANE!f9F s{ •::21.~.:tANFl9t
GW/ChemW
GW/ChemW
S VO/8260
S WC/TOC
REF.126-1 *l
REF 121-1 *2
PH Remarks
~---
1;990•++.50:2fp1/ {$):i"R-••·•c$t:gp~1tt>•••• ·•···•·•·•·•·•······\ l4S4'ANS9 .• 9T!;ti/4$ t·4tJAN.¥99!$//:27P.rANESJ.•9/
Leachate
Leachate
Leachate
Leachate
Leachate
Leachate
Leachate
Leachate
Leachate
Leachate
Leachate
Leachate
Leachate
Leachate
S OP/TCLP/ZHE
S OP/TCLP/EXT
S VO/TCLP
P TM/TCLP
C TM/AG/TCLP/6010
C TM/AS/TCLP/6010
C TM/BA/TCLP/6010
C TM/CD/TCLP/6010
C TM/CR/TCLP/6010
C TM/HG/TCLP/7470
C TM/PB/TCLP/6010
C TM/SE/TCLP/6010
S PS/TCLP/HERB
S PS/TCLP/PEST
REF 126-1 *l
REF 121-1 *2
REF 126-1 *3
RM 121 *4
REF 121-1 *5
REF 121-1 *5
PH Remarks
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Signatur ~ li~\-~4 !r:f Dal
000125 I
LOGIN REPORT (lnOl)
Jan 19 1999, 02:16 pm
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Login Number: L99011502
Account: HNAHOL-SHE HNA HOLDINGS INC.
Project: 60885.00 GW ,S&A REPLACES 60603.00
reach~te ·•·••·•• S•• SV /TCLP
· L9.9Q;t;t5 .. Ql.:;;Q.!3i \1'$\111 r·•••t//•.•.i•···· ..
IGW/ChemW S V0/8260
REF 121-1 *5
REF 126-1 *l
REF 121-1 *2 GW/ChemW P SV/8270/TCL+DOW
GW/ChemW. C SV/8270/BNA/TCL
GW/ChemW C SV/DOW
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PH Remarks
I GW/ChemW S V0/8260
GW/ChemW P SV/8270/TCL+DOW
GW/ChemW C SV/8270/BNA/TCL
GW/ChemW C SV/DOW
I I1.Q})Q'i:i592f:J)'i •••• {PEWH41DtJP)
GW/Chemw S V0/8260
I GW/ChemW P SV/8270/TCL+DOW
GW/ChemW C SV/8270/BNA/TCL
GW/ChemW C SV/DOW
REF 126-1 *1
REF 121-1 *2 t1A +--
••• \f4··f.JANfQ.9\:J)2IL08/\t4•·s;:rANf9•9L$ J 27½YANkQ.9U
REF 126-1 *1
REF 121-1 *2
PH Remarks
4A +--
I I19,9Ql:15Q.22Ji.2i?•····· t•l'E,W&3/{,••·······•··• ··••·••·•··•·•·····••?••·•···<)X•··•·· ++•·· l4EiJAN.S·99 X'??•.I-'?{],4f<IANH9.Q.( ... §ff\27PJAN99.9)
PH Remarks
GW/ChemW S V0/8260 REF 126-1 *l &A
I GW/ChemW P SV/8270/TCL+DOW REF 121-1 *2 =1=
GW/ChemW C SV/8270/BNA/TCL
GW/ChemW C SV/DOW ===============
I L990ll5'02.Wi3)
Leachate S OP/TCLP/ZHE
I Leachate S OP/TCLP/EXT
Leachate S VO/TCLP
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00012G
LOGIN REPORT (ln0l)
Jan 19 1999, 02:16 pm
Login Number: L99011502
Account: HNAHOL-SHE RNA HOLDINGS INC.
Project: 60885.00 GW,S&A REPLACES 60603.00
f(j,Jilfl!li1liljj;\!lli1Jii!µ\jij;i§p/I;HI --i-,i 'B!:!e~.t,:, ,:_,,'.' .':::; ;:-,,:~~i:! \111'.~iii:lill;i!Hl!!!i;i!!1
Leachate
Leachate
Leachate
Leachate
Leachate
Leachate
Leachate
Leachate
Leachate
Leachate
·Leachate
Leachate
GW/ChemW
GW/ChemW
GW/ChemW
P TM/TCLP
C TM/AG/TCLP/6010
C TM/AS/TCLP/6010
C TM/BA/TCLP/6010
C TM/CD/TCLP/6010
C TM/CR/TCLP/6010
C TM/HG/TCLP/7470
C TM/PB/TCLP/6010
C TM/SE/TCLP/6010
S PS/TCLP/HERB
S PS/TCLP/PEST
S SV/TCLP
RM 121 *4
REF 121-1 *5
REF 121-1 *5
REF 121-1 *5 -
ii t Li{ {i4.PJAft.E9Qif3!·4.4 :i.4.f;[Aftf9QI$ F••2.1/JM.2·9·9)•··
PH Remarks
S VO/8260 REF 126-1 *1 -'YA
>tt .. H>• +4.%JAftf 9Q}.,J,i4.H'.31 }14.SJNJEQQ .s/J2.7HJAft£9.9)
PH Remarks
S VO/8260 REF 126-1 *1 IV'A
.......... · ...... ·.··•·•·····.·•·····•·•···•···•·••··.·ii ..• i·•• <···•·•• '.i+ s.scr@f $$,!$ ... /f'·s•·2 crM+•·99\?
S VO/8260
PH Remarks
REF 126-1 *1 /IQ/
Page 3
000127
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DJ\VIS
FLM!D
(NCINCERS
PLANN(RS
ARCHITECTS FIELD DAT A LOG
SO(NJISIS
CHARl.ESTQH • CR(£HWOOO • COLUMBIA
FOR GROUNDWA TEA SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
Well No· ,4 ,4-.::,~ ..
croent:,/bl/A' d/d.!2j-£ -h?c:. 'Source(,_) of Well ID M,±.e 10 Lobeld§)'no) ,
Site Name: 9e/J,, ,1/C. Job Ho~.?t'f'J-).oa Well Ccmplelion: Proleclive Ccsin~/no) Rush (yes~
/ )
Date: /-J-/-t7tf LWR submilted by: nush-llounl Co-ler Seel lntod (yes/no) locki,;g Cap (f;t/no)
Sampling Personnel: ✓-lrr $h.t_ locked al Arrivcl{§j)/no) Departure!:!3Jno)
'
S-d• Personne~ ./4./' .C ;,f,,,,,L, .{a. L Well Ccsinr(n"•igh~depth below) greund: t s--!I,
Regulatory Personne~ -Casing Type (PVC) ~) (other)
Weather Ccndittons: Cleo r: Temp.:t'O ~or Boner (yes/M) Type
Well Diameter. 2,0 In. Protec live Post/ Abulmcnt (yeshfil) Concrete Po~/no)
(A) Top of Well Devotion: zzg_ 1/4· msl (yes/no) Well Integrity SolisfocloryBno) ti no, explain below.
(8) Depth to Immiscible Loyer: -ft. Well Yield ( low / moderate / ~)
(C) Immiscible Loyer Etevotion: (A)-{B)= -msl (yes/no)
(0) 0eplh to Groundwoter. :JS. " ✓ ft. W£ll VOLUME DATA
(E) Groundwater Elevolion: (A)-{D)= C 9 3 , I Z msl (yes/no)
DIA. OF PIPE (in.) VOLUME IN GAL/Fl.
1.0 0.041
(F) Totol Well Depth = £"/0 It. 2.0 0.163
3.0 0.367
(G) length of Woler Column: (F)-(D)= lif..~l ft. 4.0 0.653
' 5.0 1.020
Casing Volume = (G) x Volume in gol./ft.= s. l gals. 6.0 1.470
'
Method of Wen Evocuofion £1 I,,:;,.,,,., /) Slorf Time: K'Z-4 TO CONVERT GAL/n TO UTERS/n. MULTIPLY ABOVE FIGURES BY
r I 3.8 LITERS/GALLON. .·
Method of Sample Colleclion t?t =,£) Time:/ >'./..8
I
Choin-of-Cusio<iy Form Started @no)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged (gallons) 3. I L "2-'7. '?
Time (mmlory) ., ~,,? V i.:,~ 5 ,.,-,;7 .
pH (S.U.) :, • '2. 6-1. =-,
Sp. Cond. (umhos/cm) .J,{ 'I '? ,c q 3 ,,( q
Waler Teinp. (•c) 15" ts /< :
Odor (subjeclive)• . I I I
Turbidity (subjeclive)•• , I I
• (!)Hone (2)Slight (3)1.toderole (4}Slronge
" (l)Cteor (Z)Sfightly Turbid (3)Moderolely Turbid ( 4)Very Turbid (5)Extremely Turbid
Commenls/Observations/Recommendations: ----------------------------
OAT[: . h°i--f' f
o& r rorm•S (3/9•)
000128
Df\J/1S
FLOYD
CNCIHCERS
PLANH(RS
ARCHITTCTS FIELD DAT A LOG
SODITISIS
c:HARLESTON • GREENWOOD • COLUMBIA
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
Well No -C-'-} '1.-..
Client:,,011'4 ,d/4,/'7-,;. ~c •Source{,) of Well ID Md c?. to Lobel {6;¥no) •
Site Nome: <"lre/J., Af.C'. Job No.:6'<'¢J-),oo Well Completion: Protective Cosin~/no) Rush {yes/iilll
/7
Oa1e: /-J1-1f LWR submitted by: Rush-Mount Cover Seal lnlod {yes/no) locking Cop (1,i/ no)
Sampling Personnel: ./,(, rt $ t, L. , Locked al Arrival ®/no) Departure ~no)
Sit• Personnel: /4./' J' ~,.,,,,£.fa L -Well Cosing (Sli•tgh~/deplh below) ground: 9-o fl,
R09ulolory Personne~ -Cosing Type~{Sleei) {other)
Weather CondiHons:OQ e i:: c_a. ~./-Temp.: 11Jj_ ~ or Bo~er {yes/no) Type
Well Diameter: 2.0 in. Protective Post/Abulmenl~no) Concrete Podd9/no)
(A) Top of Well O.volion: %6. +. Ll msl {yes/no) Well Integrity Solislodory @/no) If no, explain below.
{B) Depth to Immiscible Loyer. -fl. Well Yield (low/ moderate/@
{C) Immiscible Loyer Devotion: {A)-{B)= -msl {yes/no)
(0) Depth to Groundwater. L 7,o<'. ft. WELL VOLUME DATA
{[) Groundwater Elevation: {A)-{D)= msl (yes/no)
DIA. Of PIPE (in.) VOLUME IH GAL/fl.
1.0 0.041
(f) Total Well Depth = 4'l..,.oo ft. 2.0 0.163
JL ti 3.0 0.367
{G) Lenglh of Waler Column: {F)~(D)= ft. 4.0 0.653
5.0 1.020
Cosing Volume = (G) x Volume in got./ft.= 1:.10 gals. 6.0 1.470
.-
Method of Well [vocuofion L/lbn7{Z_ Sfort Time: /65''--/ TO CONVERT GAl/fT TO UTERS/FT, MULTIPLY ABOVE FlGURES BY
. ~ , ' 3.8 LITERS/GALLON .
Method of Sample Collection a,.,/'U"I./J Time: //z_ / I I
Chain-of-CusiOOy form Started @no)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Vokane 4th Volume 5th Volume
Volume Purged (gallons) .,. i '"·-(" / !i.'
Time (mmtory) }/6 Z II 11 I 1 • 0 .
pH {S.U.) s. 3 .:,: ,_ <r. f
Sp. Cond. {umhos/ cm) 2<" > > z'
Waler Temp. (·c) /7 /7 I 7 :
Odor {subjective)• -I I '
Turbidity (subjective) .. I I '
• (1)None (2)Slighl {3)Moderole (4)Sfronge
" (1)Cleor (2)Slighfly Turbid {3)Moderolely Turbid (4)Very Turbid (S)Extremely Turbid
Commenls/Observolions/Recommendalions: ------------------------------
OAtl 1-14':1f1
D& r form48 (J/94)
000128
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I DI\JIIS
I FLOYD
[HCINHRS
PLAHNCRS
ARCHITECTS
SODl(IS1S
FIELD DATA LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
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ARLESTQN • <?REEt~WOOO • COLUMBIA Well No· <-C-s 3 .. .....
Client,,,lbt/4 .dd&J-~ /4c. 'Source(,) of Well 10 M,:t_P IO lob el /;Gino) •
Sile Home: </,e/)., Af.C. Job Ho~.(,:,¢J-).oo Well Completion: Protective Cosing~/no) flush (yes~
f)
Date: /-Ji-t7'f lWR submilled by: flush-Mount Cover Seel lnlod (yes/no) locking Cop<(fjs/ .G)
Sampling Personnel: ✓~n dlu.z. , locked cf Arrivol~/no) Departure (t.iµ,o)
Sil• rersonnel: ✓,,.{',( ~,,,/4.f,/ Well Cosing ~depth below) ground; c..S-11,
Regulcfory Personnet -Cosing Type (PVC~ (other)
Weather CondiHons: tP u f' ~<L .;;,,_, Temp.: :Z:D ~~or Boiler (yes/no) Type
Well Oiomeler. z,D In. Protective Post/ Abulmenl (ye~ Concrete Po<J@no)
(A) Top of Well Elevation: 31 Z, t? msl (yes/no) Well lnlegrily Solisfodo~o) If no, exploin below.
(B) Depth lo Immiscible layer: -fl. Well Yield ( low / moderate / high )
(C) Immiscible Loyer Elevation: (A)-(B)= -msl (yes/ no)
(0) Oeplh fo Groundwater: Z ~-3 6 fl. WELl VOLUME DATA
(E) Groundwater Elevation: (A)-{O)= Jefq. 3 0 msl (yes/no)
DIA. Of PIPE (in.) VOLUME IN GAL/fl.
1.0 0.041
(f) Total Well Depth = ,3_ 3, 0 0 ft. 2.0 0.163
q. C <--{ 3.0 0.367
(G) lenglh of Woler Column: (f)~(D)= fl. 4.0 0.653
5.0 1.020
Cosing Volume = (G) x Volume in goi./ft.= !_,0, gals. 6.0 1.470
' Start Time: f.? Z-4' Method of Wen [Y<JCUofion 12'-kkn a TO CONVERT GAl/fT TO UTERS/fT, MULTIPLY ABOVE FIGURES BY
· I I 16_>?-
3.8 UTERS/GAllON. .·
Method of Sample Coiieclion _,,,=P Time:
Chain-of-Custody form Sloe /SJ}/no)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Voklme 4th Volume 6th Voklme
Volume Purged (gollons) /, C :i, z_ 4/_y
Time (mmlory) //?3 <I Ir? 4 I I tf ~,, .
pH (S.U.) &, 3 f.. . z ,,;_-:,
Sp. Cond. (umhos/cm) l.J ( t./ LI/ b <// <r
Waler Teinp. (·c) I ,;;, /p / -6 :
Odor (subjective)' z 7' 7
Turbidity (subjedive)•• I I I
• (l)Hone (2)Slighl (3)1,!oderole ( 4)Slronge
" (1)C1eor (2)Slighlly Turbid (3)Moderolely Turbid (4)Very Turbid (S)Exlremely Turbid
Commenls/Observafions/Recommendalions: -------------------------
FORM COMPL£1(0 BY: ________ _
<-""'' OAT(: ________ _
O& f form48 (3/94)
000130
I
[NCINE[RS ARCHITECTS FIELD DATA LOG Df\YIS
FLOYD PUNHCRS SOCtl11S1S FOR GROUNDWATER SAMPLE COLLECTION/ I
GROUNDWATER ELEVATION MEASUREMENTS
CHARLESTON • GREENWOOD • COLUMBIA Well No· cc-S.Y ..
Client:~ 4 /4 /d: C?j-E-~c.. · Source(~) of Well ID !:id. e. 10 Lobel~no) •
Site Name: <lze/j,, Af:C. Job Ho~i(d¢J-).oa Well Completion: Protective Casin~/no) nush (yes/~
/7
Oaf•: /-I"/-'ff LWR submitted by: nush-l,lounl Co-,er Seal In lad {yes/ no) Locki,;g Cap !.@/no)
Sampling Personnel: J,(_ ,rl df "1.z. , Locked at Arrival (di;/ no) Departure cf.il)/ no)
. . </4./' )'.' /& n,,,/4 .fa ,{ Well. Casing ~1/deplh below) groond: --Sit• Personne~ ?.> II,
Rejjulalory Personne~ Casing Type (P.VC) ~ (other)
Weather Candifions: C:&-,, ,,_48 Temp.:iO j ~edic<lfed ~p or Bailer (yes/no) Type
Well Diameter. -;?-· In. Protective Post/ Abutment (yes/:5) Concrete Pad,®/no)
(A) Top of Well Devotion: ze?<-1. 4 fl msl (yes/no) Well Integrity Solislocfory @/no) If no, explain below.
(B) Depth to Immiscible Loyer. -fl. Well Yield (low/ moderate/~
(C) Immiscible Loyer Elevation: (A)-(B)= -msl (yes/no)
(0) Depth lo Groundwater. 2_6. :, <'? ft. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(D)= 7 ;-7, <f msl (yes/no)
DIA. Of PIP£ (in.) VOLUME IN GAf../fl.
1.0 0.041
(f) Toto! Well Depth = ..,-8,oo ft. 2.0 0.163
3.0 0.367
(G) Length of Waler Column: (f)-(D)= Zr-'--12.. ft. 4.0 0.653
-----
5.0 1.020
Casing Volume = (G) x Volume in gat./ft.= ?'-J gols. 6.0 1.470 .-
Method of WeU Evacuation n,errp Start Time: / "5/ 7 TO CONVERT GAL/IT TO UTERS/IT, MULTIPLY ABOVE flGURES BY
. I
Time: / )>¢~{_
3.8 LITERS/GALLON. .·
Method of Sample Collection 4 '¥
I
Chain-of-Cusiody form Started tf3,'no)
FIELD ANALYSES
Isl Volume 2nd Volume 3rd Voklme 4th Volume 6th Volume
Volume Purged {gallons) z -J,./ '7-& I .!J-_;,
Time (military) I 3 2-?--. I~ J z._ I J 4 z. -
pH (S.U.) [ .«T /4 _..,., t. :,
Sp. Cond. (umhos/cm) t:/7 '13 q ?
Water Temp. (•c) 17 / 7 I 7 ,
Odor {subjective)• I I I
Turbidity (subjective)•• I I l
• (l)None (2)Slighl (3)Moderole (4)Stronge
" (l)ctear (2)Slighlly Turbid (3)Moderolety Turbid ( ( )Very Turbid (5)Exlremely Turbid
Commenfs/Observotions/Recommendalions~ ------------------------------
000131
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CNGINEERS ARCHITTCTS
PLANNERS SctCHllSIS
FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
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CHARLESTON • GREENWOOD • COLUMBIA Well No · h_s:.:;-..
Cfient:,h'd4 4/41.c!j-~ ..07<!: 'Source{s) of Well ID /11-:1.e. ID Lobel~no).
Site Nome: <1,e/4,, Af.C. Job No~6c:'VJ-)-oo Well Complelion: Protective Cosing@ no) Rush {yes/{§)
/I
Dafe: /-/f-,ZtJ LWR submilled by: Rush-Mount Cover Seo I lnlocf (yes/ no) Locking Cop {yes/ no)
Sampling Personnel: J.,(.,,-t $/&_ , Locked o1 Arrival (yes/,(/{J Deporture {yes/e!})
Sitt Personne~ ./4./'..C /4--7,,,/,.faL Well Cosing ~deplh below) gr6!lnd: y_ D a.
Regulolory Personne~ -Cosing Type~ {Sleel) (other)
Weolher Condifions: tJu~c.<'t:t.~-f Temp.:Jf'~ ~dicol~or Boiler /:Jes/no) Type
.z,.D Well Diameter. in. ,unec11ve Post/Abulment@no) Concrete Pod~no)
(A} Top of Well Oevolion: "84£ I~ msl (yes/no) Well Integrity Salislocfory~/no) If no, explain below.
(B) Depth to Immiscible Loyer. -fl. Well Yield ~ moderate / high )
.
(C) Immiscible Loyer Devotion: {A)-(8)= -msl {yes/no)
{D) Oeplh lo Groundwoler. JS'.l_✓ ft. W(LL VOLUME DATA
{E) Groundwater Elevolion: {A)-(D)= fi' t!D>....--ms! (yes/no)
DIA. OF PIPE {in.) VOLUME IN GAL/Fl.
1.0 0.041
(F) Tolol Well Depth = ::r5:&0 fl. 2.0 0.163
3.0 0.367
{G) Lenglh of Waler Column: {F)-(D)= / c. ,,:1' fl. 4.0 0.653
5.0 1.020
Cosing Volume = (G) x Volume in gol./fl.= 2-,. "ff gals. 6.0 1.470
.-
Method of Wen Evocuafion ,<")~~~.a. Start Time: d;t,;/0 TO COHV!:RT GAl/fT TO LITERS/FT, MULTIPLY ABOV£ FlGIJRES BY
. r~ 3.8 LITERS/GALLON, ·
Method of Sample Collection /1, . •f Time: Ueq z
Choin-of-Cusiooy Form Started @no)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged (gallons) 0/?Yr?D Id
Time {mnilory) o 1'f7
.
pH {S.U.) s: 'r
Sp. Cond. {umhos/ cm) < C, i
Waler Temp. (•c) ? z._.. :
Odor {subjective)• 4
Turbidity (subjective)" 7
• (l)Hone {2)Slighl {3)Moderole (4)Slronge
" (l)cleor (2)Sfightly Turbid {3)Moderolely Turbid {4)Very Turbid {S)Exlremely Turbid
Commenls/Observotions/Recommendalions: ------------------------------
000132
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[NCINE(RS ARCHrrtCTS FIELD DAT A LOG Df\YIS
FLfrfD Pu.NHERS SctCHltSTS FOR GROUNDWATER SAMPLE COLLECTION/ I
GROUNDWATER ELEVATION MEASUREMENTS
CHARLESTON • GREENWOOD • COLUMBIA Well No · /.,C-: ..3 ~ ..
Cli,nl:,/bl/4 /-/4MC!f-£ -h?<=-'Source{s) of Well ID !::i.d.e ID lobel~/no) •
Sile Home: <ize/)., A(C. Job Ho.:{t19'.,C),oo Well Complelion: Profeclive Cosin~/no) Rush {yes/~
/ J
Dale: /-J-/-4_'f LWR submilted by: nush-Mounl Cover Seol lnlact (yes/no) locking Cop (fe}/ no)
Sampling Personnel: ✓-<.rt $JAL , Locked at Arrivo~ no) Departure {~o)
Sil• Personnel: /4:/' j' ;,,& ,,,,,/4 .fa. -' -Well Cosing ~/deplh below) grclllnd: ?.D fl,
Regulatory Personnet Casing Type (PVC) ~ {other)
Weolher Conditions: c:1/ &1,... Temp.: fo'2 @ca~~ or Bailer (yes/no) Type
Well Diameter. 2. D In. Proleclive Posl/ Abulmenl {yes/ ,ff) Concrete Pad Jji9/no)
(A) Top of Well aevofion: 777., 73 msl (yes/no) Well lntegrily Solisfodory ~no) If no, exploin below.
{8) Oeplh to Immiscible layer: -fl. Well Yield (8)/ moderate / high )
(C) Immiscible Loyer Elevation: (A)-{B)= -msl (yes/no)
(D) Deplh lo Groundwaler. !.."'-'7 fl. WELL VOLUME DATA
{[) Groundwater Elevolion: (A)-(D)= Zt" .l 1 0 t msl {yes/no) DIA. OF PIPE {in.) VOLUME IN GAL/fl.
' 1.0 0.041
(F) Total Well Oeplh = 3L/;s-o f I. 2.0 0.163
7'3.153
3.0 0.367
{G) Length of Waler Column: (F)~(D)= fl. 4.0 0.653
J,'1 5.0 1.020
Casing Volume = {G) x Volume in gal./11.= gals. 6.0 1.470 _.
Start Time: / ~ 2-(. Method of WeU Evacuation e.u-xrya TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABO¥£ FIGURES BY
I 3.8 LITERS/GALLON. .·
Melhad of Sample Collection £)_ I vns<J Time: /65.:>
I
Choin-of-.Cusiooy Form Slorfed ~/no)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume •th Volume 6th Volume
Volume Purged (gallons) "-Lo ,PvA'i>Z.tl/
.
Time {mTiilory) /,< SC / t,; 'l'-6 .
pH (s.u.) [d c. )
Sp. Cond. (umhos/cm) S-f ,c· I
Waler Temp. ("C) /,( , ( ,
Odor {subjeclive)' I I
Turbidily (subjective)" I I
• (1)None (2)Slighl (3)Moderate (4)Slronge
" (l)cteor (2)Srighlly Turbid (3)Maderalely Turbid ( 4 )Very Turbid (S)Exlremely Turbid
Commenls/Observotions/Recommendofions: ------------------------------
O& r form48 (3/94)
000133
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Df\J/1S
FLOYD
CNCINHRS
PLANNERS
ARCH(T[CTS
SCtDIHStS
FIELD DAT A LOG
FOR GROUNDWA TEA SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
CHARLESTQH • CRECHWQQD • COLUMBIA Well No.: /'" ,,t::::-:;{' c.
crient:/2'.fa""A ,d,/dC!j-€. /4~ • Source(s) of Well ID Md.,,, ID label ~no) •
Site Name: ge/J., A/.C. Job No.:6tl¥.,S-,).ao Well C<>mplefion: Protective Casin~/no) flush (yesh!o}
I I
Dale: /-/1-t?dJ LWR submitted by: flush-Mount Cover Seal fnlad (yes/ no) Locki,;g Cap ~/no)
Sampling Personnel: ✓«rr /.#uL. , Locked a1 ArriV<>I {9s/ no) 0.parture ~no)
S"dt Personnet /4./'.l' ~a,/4faf Well Casing ~Ydeplh below) gr<Xind: 3'.o (I
Regulatory Personnel: Casing Type (PVC) ~ (other)
{_'/-,.ui,::_ -I ~or Boiler (yes/no) Type Wealher C<>ndiUons: Temp.: ~ ,:2_ ~
WeU Diameter: z.D In. Proleclive Post/ Abutment (yes/<fij;J, Concrele Pod {i;.l/no)
(A) Top of Well Devotion: 77Z I f msi (yes/no) Well Integrity Solisfoctory ~/no) If no, explain below.
(8) O.pth lo Immiscible Loyer. ~ fl. Well Yield (<!£:I moderate / high )
(C) Immiscible layer Elevation: (A)-(8)= -msl (yes/no)
(0) Oeplh to Groundwater: //. 1..'l fl. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(0)= 7 6/_ t>G' msl (yes/no) DIA. or PIPE (in.) VOLUME IH GAL/fl.
1.0 0.041
(f) T olol Well Oeplh = .< c-✓o f I. 2.0 0.163
3.0 0.367
(G) Length of Waler Column: (r)~(D)= ,17 t, z l fl. 4.0 0.653
;r. ] 5.0 1.020
Casing Volume = (G) x Volume in gal./fl.= gals. 6.0 1.470 ..
Method of Wen EV<>CUofion /)/ l::%27'2-Start Time: /~5-0 TO CONVERT GAL/FT TO UTERS/fT, MULTIPLY ABOVE FlGURES BY
I 3.8 LITERS/GALLON. .
Method of Sample Collection PC!ay:2 Time:/! J/7
I
Chain-of-Cusiooy form Started (ii}-/no) .
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged (gallons) Y. .3 ,,,,,<i/4\ I ,r-,-
lime (mmlary) /¢0< 16 ·z,. ,-
.
pH (S.U.) (.. ,z. (,,. ~
Sp. Cond. {umhos/cm) .x I 1( D
Waler Tef11p. (•c) I£ 1~ r
Odor (subjeclive)• I I
Turbidity (subjective)" I I
• (l)Nane (2)Slighl (3)1,iaderole (4)Slronge
" (l)cleor (2)Slighlly Turbid (3)Moderolely Turbid (4)Very Turbid (S)Exlremely Turbid
Commenls/Observations/Recommendalions: ----------------------------
. (SO!ATUR()
061, ,~, q-r'l
O& r form48 (3/94)
000131
I
(NCIH((RS ARCHITTCTS FIELD DATA LOG Df\J/1S
FLOYD PLANN(RS SCl(HllSTS FOR GROUNDWATER SAMPLE COLLECTION/ I
GROUNDWATER ELEVATION MEASUREMENTS
CHARLESTON • GREENWOOD • COLUMBIA Well No·&-&-;( J ..
Cf1<11t:ffi!/4' ,d/4t'7"£ -,0?c. 'S.urce(s) of Well ID M-:J. r!!. ID label ~/no) •
Sile Name: ;(/,e/)., Al. C. Job No.:.( t19'.J-). o a Well Completion: Protective Cosin&s/no) flush (yes/c!fo) r1
Date: /-If-t:JtJ LWR submitted by: flush-Mount Cover Seo! Intact (yes/no) Locki.;g C<ip ~/no)
Sampling Personnel: J/4..M $tr.!. locked al Arrivo~no} Oepcrtur~ no) ,
S"de Personne~ ./4 .I' .c ~ ,,.,,,/4 .fa. ,{ . WeU Cosing~/deplh below) gr6und: 3 fl,
Regulatory Personnel: -C<islng Type (PVC)~) (other)
Weother C<indilions;/4',:4 a& /7 Temp.: t{a 5 <!§ficate8 $P or Boner /Jes/no) Type
Well Diameter. 2.0 in. Protective Post/Abutment (yes/G;j C<increle Pod ~no)
(A) Top of Well Devotion: 2 7,!_, 7p msl (yes/no) WeU Integrity S.lisfoctory (yes/no) If no, explain below.
(8) Depth lo Immiscible Loyer: --fl. Well Yield ( low/ moderate /@)
{C) Immiscible Loyer Elevation: (A)-(B)= -msl (yes/no)
(0) D•plh lo Groundwater: I f?,t ;/ fl. WELL VOLUME DATA
'
(E} Groundwater Elevation: (A)-(D)= 7.5J,;"f msl (yes/no) DIA. Of PIPE (in.) VOLUME IN GAL/fl.
1.0 0.041
(F) Total Well Depth = ti. oo fl. 2.0 0.163
• 3.0 0.367
(G) Length of Woler Column: (F)-(D)= '12'. J £ fl. 4.0 0.653
~-'1 5.0 1.020
Cosing Volume = (G) x Volume in gol./11.= gols. 6.0 1.470 ..
llelhod of Wen Evacuation OJ.g~Q_ Start Time: 14 4-f TO CONVERT GAi/FT TO LITERS/FT, MULTIPLY ABOVE FlGURES BY
7 ~ 3.8 LITERS/GALLON. ,,
Method of Sample Collection O{.f_-:1:3 a Time:/,-I 8'. r I
Choin-of-CusiOOy form Storied @/no)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 6th Volumo
Volume Purged (gallons) 7.,:!, /L,I,,:;, .'7 I n
Time (military) / L/ -~-z._ / <>, ,l ;:,,/ .
pH (S.U.) /..4-~~ c, 3
Sp. Cond. {umhos/cm) IC? L I Z 1 I 7: '7
Waler Temp. (•c) // ft. /" ,
Odor (subjective)• I I I
Turbidity (subje<live)" I I I
• (1)None (2)Slighl {3)Moderole ( 4)Slronge
" (l}cleor (2}Slighlly Turbid (3)Moderolely Turtid (4)Very Turbid (5)Extremely Turtid
Commenls/Observations/Recommendalions: ----------------------------
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O& f form48 (3/94)
000135 I
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(NCINECRS ARCH(T(CTS FIELD DAT A LOG
PLANH(RS SCIEHHSTS FOR GROUNDWATER SAMPLE COLLECTION/
DAJ.11S
FLOYD
CHARl.£STOtl • CRECtlWOOO • COLUMBIA GROUNDWATER ELEVATION MEASUREMENTS ,/
Well No • ,t,//.1-,-Y ..
cr .. nt:,#A/4 44,, -h?<!C-Source(,) of Well ID M,1:e ID Lobel ~no) •
Site Home: de/)., ,Al'.C. Job Ho~.?,::,si;c)-oo Well Completion: Proleclive Cosing§lno) flush (yes/@
r;
Da1e: /-If-4-J LWR submilled by: flush-Moun! Cover Seal lnloct (yes/ no) locki.;g Cop {i;lr./ no)
Sampling Personnel: J,(_ ,rl $h,,t_ Locked o1 Arrival (.,B/no) Deporture~/no) ,
Well Cosing~/deplh below) ground:
Site Personnel: /4./' ..C ~,,,,/, .fa L 2::.S-II,
Regulatory Personnel: -Cosing Type (PVC) (~ (other)
Weather Condifions: auc:rce:. sJ ::t£.' Temp.:~} ~£;;, or Boner (yes/no) Type
Well Diameter: Z,O In. Proleclive Post/ Abulmenl (yes/~ Concrete Po~/no)
(A) Top of Well Oevolion: 75'.S-: qi_ msl (yes/no) Well lnlegrily Sotisfoctory~/no) If no, explain below.
(B) Depth to Immiscible Loyer. -fl. Well Yield ( low / ~ / high )
(C) Immiscible Loyer Elevation: (A)-(B)= -msl (yes/no)
(D) Deplh lo Groundwoler. -,lo,;D fl. Wtll VOLUME DATA
(E) Groundwater Elevation: (A)-{D)= ?IL/, f-</ msl (yes/no)
DIA. Of PIPE (in.) VOLUME IH GAL/fl.
1.0 0.041
(F) Total Well Oeplh =. Ljf<', (17c) II. 2.0 0.163
3.0 0.367
(G) lenglh of Waler Column: (f)~(D)= '-..) -fl. 4.0 0.653
5.0 1.020
Cosing Volume = (G) x Volume in gol./ft.-L-Z-gals. 6.0 1.470
'
li~thod ol w,n E="!i•n /t.vtcnf2 Siar! Time: ti q ..-_; -TO CONVERT GAL/IT TO UTERS/IT, MULTIPLY ABOVE FIGURES BY
3.8 UTERS/GAUON. ·
Mel hod of Som pie Collection AJ I t'!::'¥2 Time:('.p ':l_ -4
;r (§ii Choin-of-Cusio<iy form Slorled /no) _
FIELD ANALYSES
1st Volume -12nd Volume 3rd Volume •th Volume 6th Volume
Volume Purged (gallons) I I 2. , . -. ~ -l>iJVl,J?'/y•
Time (mmlory) /o•o IOt?tf /61'-I .
pH (S.U.) ,· ,U ,·. D /. ,: t7
Sp. Cond. {umhos/ cm) / (' /.,; " 1
Waler Temp. (·c) ,~ ,~ I/ '
Odor (subjective)' . I j I
Turbidity (subjective)" I , I
• (!)None (2)Sligh1 (3)Moderole (4)Slronge
" (1)Cleor (2)Slighlly Turbid (3)Moderolely Turbid (4)Very Turbid (S)Exlremely Turbid
Comments/Observolions/Recommendolions: ----------------------------
DA,✓ I-( t/ ':ff
O& r focm48 (3/9•)
00013G
I
(NCJN((RS ARCHITECTS FIELD DAT A LOG Df\J/1S
FLOYD Pl...ANN(RS SOCHllStS FOR GROUNDWATER SAMPLE COLLECTION/ I
GROUNDWATER ELEVATION MEASUREMENTS
CHARLESTON • GREENWOOD • COLUMBIA . Well No · ///1-7 7 ..
Cfo,nt:jbl/4 /k/d°7£ -h?~ · Source(,) of Well 10 Md.. t!!. 10 Lobel ~no) •
SIie Nome: <lze /)., Af. C. Job No~ 6,:, ¢-,-). O o Well Completion: Protective Cosin~/no) Rush (yes/6)
/7
Dale: / · l.t/-4CJ LWR submitted by: nush-llount Cover Seal Intact (yes/no) Locki~g Cop G¼' no)
Sampling Pe=nnel: J-<-n /.61£,u locked a1 Arcivald§feo) Departure 'ffejJ,,o) ,
Sitt Personnel: ✓e ./' J' ~ ,,,,,,/4 .fa L Well Cosing ~depth below) ground: 2:_;-II,
Regulalory Personne~ Cosing Type (PVC)~ (other}
Weather Condifions: ,p (,~ ,-,: ":$ f-Temp.:§ ~afe<(P? or Boiler (yes/no} Type
Well Diameter. z.t'J In. Protective Post/ Abutment (yesi!lfil) Concrete Padd@'/no)
(A) Top of Well Oevotion: ,7r.5'":' _J7 7 msl (yes/no) Well Integrity Solisfoctory~no) If no, explain below.
(B) Depth to Immiscible Loyer. -fl. Well Yield ( low / moderate ~)
(C) Immiscible I.ayer Elevation: (A)-(B)= -msl (yes/no)
(D) Depth to Groundwater: 'fO. I 1 ft. WELL VOLUME DATA
(E) Groundwater Elevalion: (A)-(0)= 7; <, { 8 msl (yes/no)
DIA. or PIP[ (in.} VOLUME IN GAL/rt.
1.0 0.041
(F} Totol Well Depth = 7z_oo ft. 2.0 0.16:l
:i.o 0.:167
(G) length of Water Column: (r)7(D}= J_t_.~J ft. 4.0 0.65:l
5.0 1.020
Cosing Volume = (G} x Volume in gol./ft.= (, 0 gals. 6.0 1.470 .-
Method of Wen Evccuotion 11.C{~.a Start Time: 10; £ TO COHVERT GAi/FT TO UT£RS/fT, MULTIPLY ABOVE FIGURES BY
I Time: {_O,/. L
:l.8 LITERS/GALLON. .
Mclhod of Sample Collection /lb? ....,.::-,,(2
r l!fi) Choin-of-Cusiooy form Storied no)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume ◄th Volume 6th Votume
Volume Purged (gallons} L . .c? I?. _, I :P. o
Time (m«ilory) 1/J 7 J /CJ Tl ,,,40 .
pH {S.U.) .,, II C. I t.J
Sp. Cond. (umhos/cm) 41 7 /7 ,...,
Waler T en,p. (' C) I t, /;( /ti '
Odor (subjective)' . I I I
Turbidity (subjective)" J , I
• (1}None (2)Slight (:l}Moderole (4}Slronge
" (l}Cleor (Z)Slighlly Turbid (3)Moderotely Turt,id (4)Very Turbid (S)Extremely Turtid
Commenls/Observofions/Recommendations:
. (SO,U.Mll) 1-r .,.,c
O& r form48 (3/9•)
000137
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Df\YIS
fL{jyD
(HCINHRS
Pl.ANH(RS
ARCHITTCTS FIELD DATA LOG
SOOUISlS
CHARL£STQH • CREEHWQQO • COLUMBIA
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
Well No.: /;:(-z 7{'
Client:,/i'.A/4 4/ate?j-:E'. -,0,?c.. 'Source(s) of Well ID ti.ef. c!. ID Lobel (&}no) •
Sit• Home: >'l,e/)., A(C. Job Ho.,,<,:,¢,.s-).oa Well Complefion: Proleclive Casing@/no) Rush (yes/4§)
/)
Dole: /-/'f-t7(j LWR submitted by: nush-Mounl Cover Seo! lnlaet (yes/ no) locking Cap<3l9/no)
Sampling Personnel: J.,(,M $/,,c,t_ locked at ArriV<>~ no) 0.parture ~/no)
'
Sit• Personnet /4./' .c RaA,/4 .f2. £ Well Casing~/deplh below) ground: 4a fl,
Regulatory Personnet -Casing Typ• (PVC) ~ (other)
Weolher CondiHons: Over L c-sf Temp.: ,---0 ~ Or Boiler (yes/no) Type
Well Diameter: Z. 0 In. Proteclive Post/ Abulmenl ~no) Concrele Pod@no)
(A) Top of Well Elevation: 'B{/.Z,t> msl (yes/no) Well lnlegrily Solisfoclory l,(f}/no) If no, exploin below.
(B) O.pth lo Immiscible Loyer: -fl. Well Yield ( low / moderate / high )
(C) Immiscible Layer Elevation: (A)'-(B)= -msl (yes/no)
(0) Oeplh lo Groundwoler: LJf.Lz__ fl. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(D)= 7 9 3 ,0'3 msl (yes/no)
DIA. Of PIPE (in.) VOLUME IN GAL/ff.
1.0 0.0~1
(f) Tolol Well Depth = Z'/5,c()O II. 2.0 0.163
Ci'-5' Fl 3.0 0.367
(G) lenglh of Woler Column: (f)~(D)= fl. ~.o 0.6S3
5.0 1.020
Casing Volume = {G) x Volume in gal./fl.= L,(:, gals. 6.0 1.470
\,
:
Method of Well [YOCUafion /Juaz, ,a Slort Time: / :z 30 TO CONVERT GAL/IT TO Ul£RS/IT, MULllPLY ABOVE FIGURES BY
r ;
Time: /7)~
3.8 LITERS/GALLON. .
Method of Sample Colleclion Ot ,,.,_.., a_ 77
Chain-of-Cusiody form Slorted @/no)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged (gallons) /. 7 3-""-ntvvv;(.,fl/
Time (mi1ilory) I 7 3 7 I 7 "'f JI!, / 7 ,-,, .
pH (S.U.) /,.. ,5 I,. 7 t, 7
Sp.· Cond. (umhos/cm) 2. ✓-A ;, ,-; 7 z /,. I,
Wafer Temp. ("C) / 7 /7 /7 '
Odor (subjeclive)• 1 3 ?
Turbidity {subjective)•• I I I
• (!)Hone (2)Slighl (3)Moderole (4)Slronge
" (l}cleor (Z)Slighlly Turbid {3)Moderolely Turbid (4)Very Turbid (S)Extremely Turbid
Commenls/Observalions/Recommendolions: ----------------------------
000138
O& r form48 (3/94)
DIQ/1S
FLOYD
ENCINCERS
PLANNERS
ARCHITCCTS
SOENTIS1S
CHARLESTON • GREENWOOD • COLUMBIA
FIELD DAT A LOG
FOR GROUNDWA TEA SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
Well ..
Cli,nt:,/bV.4' ,d/4t'7~ /4~ Source(,) of Well ID !!U.e ID label 6'?}/no) •
SHe Home: >he/)'< A/.C. Job Ha"t'"£--C)-oa Well Completion: Prateclive Cosing t.fiilna) Rush (yesTeii)
I I
Da1e: /. If-4t:J LWR submitted by: Rush-Mount Co-,,er Seal Intact (yes/no) locking Cop (~no)
Sampling Personnel: ✓-<. /'( $ L,, L. lacked of Arrival~o) Departure ~o)
'
Sit• rersonnel: /4./' /' ~,;,,,£ .fo L Well Casin.:(liei~1deplh below) ground: .3"; Q II,
Regulatory Per:onnel: Casing Type (PVC) (~ (Oiher)
. Gu.d7 g:, Temp.: 5,:J '> Oedical<d"l'tlm or Boiler (yes/no) Type Wealher CandiHons:e,
Well Diameter. 2.. 0 In. Proteclive Post/ Abulment (yes/,!§) Concrele Podc:fr.ii)'no)
(A) Top al Well Oevotion: '78'1?. / Z.. msl (yes/no) Well Integrity Solisfacto~no) If no, explain below.
(B) Depth to Immiscible layer. -fl. Well Yield ( low / maderale / high )
(C) Immiscible layer Oevation: (A)-(B)= -msl (yes/no)
(0) Depth to Groundwater. 2-¾/l fl. WEll VOlUME DATA
(E) Groundwater Elevation: (A)-(D)= Ztf,ol msl (yes/no) DIA. or PIPE (in.) VOlUME IN GAL/Fl.
1.0 0.041
(f) Tolal Well Deplh = 58,00 It. 2.0 0.163
3.0 0.367
(G) lenglh of Waler Column: (f)c-(D)= 33,Bi ft. 4.0 0.653
,,;;o-5.0 1.020
Casing Volume = (G) x Volume in gal./ft.= gals. 6.0 U70
Start Time: / / >' J? '
Method of Won Evacuotion /}ut-27;,a TO CONVERT GAI./FT TO LITERS/FT, MULTIPLY ABOVE flGIJRES BY
. I 3.8 UTERS/GALLON. .·
Method of Sample Collection 0 / / -d::.':T" rJ Time:/ 7 z i?
~ r
Choin-of-Cusio<ly Form Storied {£)/no)
FIELD ANALYSES
1st Volume 2nd Volume . 3rd Volume ~th Volume 6th Volume
Volume Purged (gallons) s-. < ()b1./A'\-, "''
Time (military) ,~ o/.. I 7 t ", -
pH (S.U.) C,>-t:' 7
Sp. Cond. {umhos/cm) .S-5-d !,-I. c}
Water Tel!lp. (·c) /X I ',f° ,
Odor (subjective)• I ' Turbidity (subjective)" / (
• (1)None (2)Slighl (3)Moderole (4)Slronge
" (l)c1ear (Z)Sflghlly Turbid (3)Moderalely Turbid (4)Very Turbid (5)Extremely Turbid
Commenls/Observolions/Recommendolions: -----------------------------
OAtl;:.u/~{~
D& f form48 (3/94)
00013~)
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DAJ.11S
FLOYD
[NCINEERS ARCHrTCCTS
PLANHCRS SCIOUISTS
FIELD DAT A LOG
CHARLESTON • GREENWOOD • COLUMBIA
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
Well No· 7-35'°' ..
esen,:,JLN' 4 d/df ay-£ /4c.. Source(s) of Well ID Md. c:. 10 Lobel ~no) •
Sile Hom<: <l,e/)., Al,C. Job Ho~{t>¢J-)-aa Well Completion: Proleclive Casingd,1s/no) Rush (yes/~
/7
Oa1e: /-/1-'7'1 LWR submill•d by: Rush-Mount Caver Seal lnlocl (yes/no) locki,;g Cap ({w'no)
Sampling Personnel: J,(_n~ , locked al Arrivol~) Oepartur~o)
Sil• Personne~ ./4../' ,c A',; ,.,,L, ,/a L Well Casinfjheight 9/deplh below) ground: 3'.S-II,
Regulatory Personnel: Casing Type (PVC) 6Jr (other)
Weather Condittons:C¼ ;,-d~ Temp.: /4o ~ @~or Boiler (yes/no) Type
Weft Diameter: ? . 0 In. Prolcclive Post/ Abutment (yes~ Concrete Pod ~/no)
(A) Top of Well Devotion: 72Z ~:,,:, msl (ye,/no) Well lnfcgrify Solisfoclory~no) If no, explain below.
(8) Depth to Immiscible Loyer: -fl. Well Yield ( low / moderofe I high )
{C) Immiscible Loyer aevofion: (A)-{B)= -msl (yes/no)
(D) Oeplh lo Groundwoler: /ft../z.. ft. Will VOLUME DATA
(E) Groundwater Elevolion: (A)-{D)= msl (yes/no)
DIA. OF PIP£ (in.} VOLUME IN GAL/Fl.
1.0 0.041
(f) Tolol Well Depth = 3-5:70 f I. 2.0 0.163
3.0 0.367
(G) lcnglh of Woler Column: (F)-(D)= 2'12 i_ ft. 4.0 0.653
3.15
5.0 1.020
Cosing Volume = (G} x Volume in gol./11.= gols. 6.0 U70
M~thod of Wen Evocuo_tton Pu~
..
Slort Time: /3 4 f TO CONVERT GAi/FT TO LITERS/FT, MULTIPLY ABOVE FlGURES BY
Method of Sample Collection Pr, ,-rn 9 Time: /~?7
3.8 UTERS/GAUON." .·
' I
Choin-of-Cusiody form Storied @no}
flELO ANALYSES
1st Volume 2nd Volume 3rd Voklme 4th Volume 6th Volume
Volume Purged (gollons) L.I_ ,:;:, JI .0 I:;,. c>
Time (mililory} /757 1,Lfo I ,l~fi .
pH (S.U.) 5.g r, 7 <:-,(
Sp. Cond. (umhos/cm) <2~ :,--2-a 5"z.o
Waler Te(Tlp. (·c) J fl I /( I 'f<' ,
Odor (subjective)• . I I I
Turbidity (subjective)•• ' I I
• (!}None (2)Slighl (3}l,loderole (4}Slronge
" (1}cteor (2)Slighlly Turtiid (3}t,toderolely Turtiid ( 4}Very Turt,jd (S}Exlremely Turtiid
Comments/Observotions/Recommendolions: ----------------------------
: ~1.-/-15'
O&: f form48 (l/94)
000140
I
CNCIHHRS ARCHrrtCTS FlaD DATA LOG Dl\_l/1S
FLOYD PLA.NN£RS SO(NllSlS FOR GROUNDWATER SAMPLE COLLECTION/ I
GROUNDWATER ELEVATION MEASUREMENTS
cHARLESTQN • GREENWOOD • COLUMBIA Well No.: V-t:? 3
Cli<nt:/i'.,V.4' /4/atC!j-£ -h?c · Source(s) of Well 10 /11,1.e. IO Lobel tf1iJt no) ,
Sile Name: >he IJ '< ,1( C. Job Ho~ t!" i'J-). o a Well Complelion: Proteclive Casing@no) flush (yes®
I ;
Dcrle: /-/f-'7.J LWR submilted by: flush-Mount Cover Seal lnlod (yes/no) locking Cap lf9'no)
Sampling Personnel: ✓~/"f $tu locked o1 Arrivo'<!riiY no) 0.porture @lo) ,
Sift Personnet ✓.,j',t' ~ev/4,f, £ WeU Casin~deplh below) grollnd: . C:~n.
Regulo1ory Personnel: ........ Casing Type (PVC) ~I) {other)
Weather CandiHons: CJ U e cr:,tL<f-€dica~r Ba~er (yes/no) Type Temp.:.;(?'
Well Oiometer. z. 0 In. Protective Posf/Abulmenl (yesl9 • Cancrele Pod~no)
(A) Top of Well Elevation: 8' ll-1 g msl {y<>/no) Well Integrity Sotis!odory lfWno) If no, explain below.
{B) Depth to Immiscible Loyer. -ft. Well Yield ( low /& high )
{C) Immiscible Loyer [levolion: {A)-{B)= -msl {yes/no)
{O) Oeplh to Groundwater. t.4-zo ft. WELL VOLUM[ DATA
{E) Groundwater Elevofion: (A)-{O)= '716.'-f CJ msl (yes/no) DIA. Of PIPE (in.) VOLUME IN GAL/ft.
z 3, ,/v 1.0 0.041
(f) Tofol Well Depth = rt. 2.0 0.163
fl-7 3.0 0.367
{G) length of Wafer Column: {F)~(D)= ft. 4.0 0.653
lA-5.0 1.020
Casing Volume = {G) x Volume in gal/ft.= , gols. 6.0 1.470
'
Method of wen Ewocuofion Ow=p Start Time: / i!f'O 3 TO CONVERT GAL/fl TO UTERS/fT, MULTIPLY ABOVE flGURES BY
. /I J?Z ,[ 3.8 LITERS/GALLON. .·
Method of Sample Collection /Jua:n/7 Time:
r@ j
Chain-of-Cusiooy form Started ye no)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged {gallons) I d ? 9 ol ,
Time (mmtory) I ,:; ·n 5 ( 6 I I ·1 gz, I .
pH {S.U.) ,t., -"f ~ /} .,._ I
Sp. Cond. (umhos/cm) /ZJ..-,. _..,-o 4 .r~-n LJ. 7/-f)
Water Tef11p. {"C) I 7 /7 I -r '
Odor (subjective)• ·1 ~ ;J
Turbidity (subjective)" I I I
• (!)None (2}Slighf (3)Moderofe (4}Sfronge
" (1)C1eor (2)Sflghlly Turbid (3)Moderofely Turbid (4)Very Turbid (S)Extremely Turbid
Commenls/Observotions/Recommendalions: -----------------------------
O& f form48 (3/94)
000141
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I DJU11S
FLOYD
ENGINEERS
PLANN(RS
ARCH(T(CTS
SQ(HIISIS
FIELD DAT A LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
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RLESTQN • GREENWOOD • COLUMBIA Well No :I-r E" ,c:-
Client/:&V4 ,d.i:,tOj-~ /4,::_ 'Source(s) of Well IO M,:1_ e. 10 Lobel (res/no) ,
Site Home: <;/,e/) v Al, C. Job Ho.: ( t' sl,,S-). o o Well Completion: Proleclive Cosing (res/no) Rush (yes/ no)
/7
Date: /-/1-4o/ LWR submilled by: nush-Mounl Cover Seol lnlad (yes/no) locking Cop {yes/ no)
Sompfing Personnel: J,<_n dffA_; locked at Arrival {yes/no) Departure (yes/no) ,
Sitt Personnet ./4./' ,/' ~--:,,,/4 .fa£ Well Cosing (heighl above/deplh below) ground: "
Regulatory Personnel: Cosing Type {PVC) (Sleel) (other)
Weother Condiffons: Temp.: Dedicated Pump or Boiler (yes/no) Type
Well Diameter. N,4 in. Proteclive Posl/Abulmenl (yes/no) Concrele Pod (yes/no)
(A) Top of Well Devotion: !:. I 6.-. msl (yes/no) Well Integrity Solisfaclory {ye,/no) If no, explain below.
(8) Depth to Immiscible layer. 6dd: fl. Well Yield ( low / moderole / high )
(C) Immiscible I.ayer Elevation: (A)-(B)= ll..! cl msl {yes/no)
(D) Deplh lo Groundwoler. •' A fl. WELL VOLUME DATA
(E) Groundwater Elevolion: (A)-(D)= NA-msl (yes/no)
DIA. OF PIPE (in.) VOLUME IH GAL/Ff.
1.0 0.041
(F) Tolol Well Depth = .6J. A f I. 2.0 0.163
3.0 0.367
(G) lenglh of Waler Column: (F)~(o)= l>l 61 fl. 4.0 0.653
5.0 1.020
Cosing Volume = (G) x Volume in gol./11.= ll,.!A-gals. 6.0 1.470
'
Method of Wen Evacuation l\.l & Start Time: Ll.!d TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOVE FlGURES BY
&:--,c;),, /13 8
3.8 UTERS/GAUON. ·
Mefhod of Sample Collection Time:
Choin-of-Cusio<ly form Storied @rno)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Vok.une 6th Volume
Volume Purged (gallons)
Time (mmlary)
.
pH (S.U.)
Sp. Cond. (umhos/cm)
Waler Teinp. ("C)
,
Odor (subjeclive)•
Turbidity (subjective)"
• (l)Hone (2)Slighl (3)Moderole (4)Slronge
" (l)clear (2)Sfighlly Turbid (3)Moderalely Turtiid (4)Very Turt,(d (5)Exlremely Turtiid
Commenls/Obsecvolions/Recommendolions: ------------------------------
-=-/'¥-((
o& r ro,m,a (3/9•)
000142
I
(NCIN[(RS ARCHITTCTS FIELD DATA LOG DAJIIS
FLOYD PLANNERS SOCHHSTS FOR GROUNDWA TEA SAMPLE COLLECTION/ I
GROUNDWATER ELEVATION MEASUREMENTS
CHARI.ESTQN • CREENWQQO • CQLUMBIA Well No.: Tt Cr_ -
Cllent,,,.01/ .4 4Ma;-..:. -h?c:. Source(s) of Well ID Md.I!. 10 label (yes/no) ,
Site Name: >he/}., A/ C. Job No~ 6 <' £'.J-). o o Well Completion: Protective Cosing (yes/no) Rush (yes/no)
/ )
Date: /-/"f-,J.J LWR submilled by: Rush-Mount Co¥er Seal lnlad (yes/no) locking Cop (yes/ no)
Sampling Personnel: J.,c ,,..-r ,$ u L.
'
Locked cf Arrival (yes/no) Departure (yes/no)
Sit• Personn•~ ./4.,{'.f' l&ac/4.faJ Well Cosing (height above/depth below) ground: "
Regulatory Personnel: -Cosing Type (PVC) (Steel) (other)
Weather Conditions: Temp.: Dedicated Pump or Bailer. (yes/no) Type
Well Diameter: N,4 in. Protective Post/Abutment (yes/no) Concrete Pad (yes/no)
(A) Top of Well Devotion: J/..4 msl (yes/ no) Well Integrity Solisfactory (yes/no) If no, explain below.
(8) Depth to Immiscible Loyer: ,,J ,4 fl. Well Yield ( low / moderate / high )
(C) Immiscible Loyer Elevation: (A)-(8)= µ4 msl (yes/no)
(D) Deplh to Groundwater: t:d.61 fl. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(D)= N,q, msl (yes/no) DIA. OF PIPE (in.) VOLUME IN GAL/Fl.
1.0 0.041
(F) Tolol Well Deplh = I\ ) A fl. 2.0 0.163
3.0 0.367
(G) Lenglh of Waler Column: (F)-(D)= ,<_) ,4 fl. 4.0 0.653
5.0 1.020
Casing Volume = (G) x Volume in gal./ft.= /l/.4 gals. 6.0 1.470
'
Method of Wen Evacuation i_J,4-Start lime: /J ,1-TO CONVERT GAL/FT TO l/T£RS/fT, MULTIPLY ABOVE flGURES BY
Method of Sample Collection &r--2--b LIL.J l
3.8 LITERS/GALLON. ..
Time:
Choin-of-Cusiod'y Form Storied ~no)
FIELD ANALYSES
1st Volume 2nd Voll.me 3rd Volume 4th Volume 6th Volume
Volume Purged (gallons)
lime (mITilary)
.
pH (S.U.)
Sp. Cond. (umhos/cm)
Waler Tefllp. (•c) '
Odor {subjective)•
Turbidity (subjective)••
• (1)Hone (2)Slighl (3)Moderole (4)Sfronge
" (l)Clear (2)Slighfly Turbid (3)Moderofety Turbid (4)Very Turbid (5)Exfremely Turbid
Comments/Observalions/Recommenda\ions: ------------------------------
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FORM COMPlIT(O BY: ~~ I
r.;;z: 1-1l';-1 I
O& r form<8 (3/94)
000143 I
I
I Df\YIS
FLOYD
(NCIN((RS
PLANH(RS
ARCHCTtCTS
SO(HIIStS
FIELD DATA LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
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CHARL£STQN • GREENWOOD • COLUMBIA Well No • .PEµ./ / .. --
Client:,/2¼"4 /-k /4£ C1j-~ /4.:.. Saurce(s) of Well ID M,£.e. ID Lobel @;no) •
S"de Name: <he/),, ,11'. C. Job Ho.: 6'" ¢,S-J. o a Well Complefion: Prolective Casing (yes/no) nush (yes/no)
//
Oaf•: /-/1-<Jt!J LWR submilled by: nush-1,founl Cover Seal lnlacl (yes/no) locking Cop (yes/ no)
Sompfing Personnel: ✓-<.n $tu lacked at Arrival (yes/no) Departure (yes/no)
'
S"de Personne~ /4./'./' /&a,/2.f,£ Well Casing (height above/deplh below) ground: "
R09ulafory Personnel: -Casing Type (PVC) (Steel) (other)
Wealher Condifions:Oo<"a:.i.t f , ' Dedicated Pump or Bailer (yes/no) Type Temp.: j"<J .I
Well Diameter: /J4 In. Proteclive Post/Abutment (yes/no) Concrete Pad (yes/no)
(A) Top of Well [levation: A£t.. mst (yes/no) Well Integrity Salisfadory (yes/no) If no, exploin below.
(B) Depth to Immiscible layer: NA ft. Well Yield ( low / moderate / high )
(C) Immiscible layer Elevation: (A)-(B)= ,I\J~ msl (yes/no)
(D) Depth lo Groundwaler. N,9_ ft. WELL VOLUME DATA
(E) Groundwater Elevalion: (A)-{D)= A/4 msl (yes/no)
DIA. Of PIPE (in.) VOLUME IN GAL/fl.
1.0 0.041
(f) Tolol Well Deplh = .IV,± ft. 2.0 0.163
3.0 0.367
(G) Length of Woler Column: (f)~(D)= N,1-fl. 4.0 0.653
JJ4
5.0 1.020
Casing Volume = (G) x Volume in gal./11.= gals. 6.0 1.470 .-
Method of Wen Evacuation µA-Start Time: -pJ A-TO CONVERT GAi/FT TO LITERS/FT, MULTIPLY ABOVE llGURES BY
C'(<,4.(3 3.8 LITERS/GALLON. .·
Melhod of Sample Colleclion Time: ll:21
Choin-of-Cusio<iy form Storied {y!no) ,·
FIELD ANALYSES
1st Volume 2nd Voklme 3rd Voklme -4th Volume 6th Voklme
Volume Purged (gallons)
Time (mTiilory)
.
pH (S.U.)
Sp. Cond. {umhos/cm)
Waler Te£11p. ("C) :
Odor (subjective)•
Turbidity (subjeclive) ..
• (f)None (2)Slighl (3)Moderole (4)Slronge
" (1)Cleor (2)51ighlly Turbid (3)Moderolely Turbid (4)Very Turbid (S)Exlremely Turbid
Commenls/Observalions/Recommendolions: {?4-,.,,,,._. ~ z,,.L ~c:/4: ~ .$@,.,...,,,,,_./;;,
---===:,__-===-===--.-';;:,,=-==:..._==/"'="'✓:,:._------
FORM COMPLETE~~-
?!7'~£..i-'2.//-~--f:z....r(c._ __
O& f form48 (3/94)
000144
I
ENCINCERS ARCHITTCTS FIELD DAT A LOG Df\YIS
FLOYD PLANN(RS SOCHIISTS FOR GROUNDWATER SAMPLE COLLECTION/ I
GROUNDWATER ELEVATION MEASUREMENTS
CHARLESTQN • CRE:EHWOOO • COLUMBIA Well No.· P.Et,u-3
I
Cfo,nt:,/2¼'4 ,/,/,«'7£ ..0?c ·Source(s) of Well ID /vi,± t!?. ID label (ij'J/no) •
S-de Nome: ,:;-/,e /j., A/ C. Job No" 6,:, ¢,,1-). Q Q Well Complelion: Protective Cosing (yes/no) nush (yes/no)
fl
Dole: /-Jf'-c7tr lWR submilted by: nush-llount Cover Seal Intact (yes/no) locki,;g Cop (yes/ no)
Sampfing Personnel: J.,(,.M$iAL. '
locked o1 Arrival (yes/no) Departure (yes/no)
Sit• Personnel: ./4./'/ /4:_~.fa.L Well Cosing (height obove/deplh below) ground: "
Regulolory Personnet Cosing Type (PVC) (Sleel) (other)
Weather C<>ndiHons: ,:2 v< r C,:, :',. /--Temp.:~ 11 Dedicated Pump or BoTier (yes/no) Type
Well Oiomefer. ;</,4.. In. Protective Post/Abutmenl (yes/no) Concrete Pod (yes/no)
(A) Top of Well Devotion: t,) !!'b msl (res/no) Well Integrity Sotisloclory (ye,/no) If no, explain below.
(B) Depth lo Immiscible Loyer: ~14 fl. Well Yield ( low / moderole / high )
(C) Immiscible Loyer Elevolion: (A)-(B)= ' 41~ msl (yes/no)
(0) Oopth to Groundwoler: /LI 4 fl. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(0)= /l) a, msl (yes/no)
DIA. Of PIP£ (in.) VOLUME IN GAL/fl.
1.0 0.041
(f) Total Well Depth = AJ-4 fl. 2.0 0.163
3.0 0.367
(G) Lenglh of Water Column: (f)~(O)= 1\)-4-fl. 4.0 0.653
5.0 1.020
Cosing Volume = (G) x Volume in gol./fl.= II l A-gals. 6.0 1.470
' '
llethod of Well Evocuofion fll.,f-Start Time: ,:'.\dA-TO CONVERT GAi/FT TO UTERS/FT, MULTIPlY ABOVE FIGURES BY
{;.RtJ.6 ./ 3.8 LITERS/GALLON. .
Method of Sample Collection Time: I Z-1 2
Choin-of-Cusio<iy form Slorled ~no)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged (gallons)
Time (mTiilory)
.
pH (S.U.)
Sp. Cond. (umhos/cm)
Waler Temp. ("C) C
Odor (subjeclive)•
Turbidity (subjective)"
• (!)None (2)Slight (3)Moderote (4)Stronge
" (1)cleor (2)Sffghtly Turbid (3)Moderolely Turbid (4)Very Turbid (S)Exlremely Turbid
Commcnls/Observalions/Recommendolions: V. .-,__, 7-. ,:./ L , A • ,,;,_L_,,. s ~;. , ,
roRM coMPI.ET£o ~Yr oW.~e:.. __ -1'_,.,_f'. __ _
O& F form48 (3/94)
000145
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I Df\YIS
I FLfilD
(NCIN((RS
Pl.ANN(RS
ARCHITECTS FIELD DATA LOG
Sct(NllSlS
ARLESTON • GREENWOOD • COLUMBIA
I
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
Well No.: ,f,' £..v _ ,/
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Client:)b1/4 At/at~~ -h?c S.urce(s) of Well ID M-±-t!!. ID Lobel ~o) ,
Sif• Name: >he II,,, A/. C. Job Ho~ 6 tJ 'IJ-). o Q Well Completion: Protective Cosing (yes/no) Rush (yes/no)
£7
Date: /-J1-cJf LWR submitted by: Rush-Mount Cover Seal Intact (yes/ no) Locki~g Cop (yes/ no)
Sampling Personnel: J,,(n /.6'1&. , Locked of ArriV<JI (yes/no) Deporture (yes/no)
Sitt Personnel: ./4./' .C i'f' ::_,L .fa L Well Cosing (height above/depth below) ground: fl.
Regulatory Personne~ Cosing Type (PVC) {Steel) (other)
Weather CondiHons:,?/J<' Kc,/ ,-,., Temp.: .:s,:, , Dedicated Pump or Boner (yes/no) Type
Well Diameter: .,-,/ d' in. Protective Post/Abulmenl {yes/no) Concrete Pad (yes/no)
(A) Top of Well Devotion: NA msl (yes/no) Welt Integrity S.lisfacfory (yes/no) If no, explain below.
(B) O.pth to Immiscible Layer: Y.4: ft. Well Yield ( low / moderate / high )
(C) Immiscible Loyer [levafion: (A)-(B)= /o./.4 msl (yes/no)
(D) Oeplh fo Groundwoler. ,,-{/4 ft. WELL VOLUME DATA
(E) Groundwater Elevalion: (A)--(0)= 11/,4 msl (yes/no) DIA. OF PIPE (in.) . VOLUME IN GAL/Ft.
1.0 0.041
(F) Totol Well Depth = #A' ft. 2.0 0.163
3.0 0.367
(G) Lenglh ol Water Column: (F)~(D)= ,N.,./ ft. 4.0 0.653
5.0 1.020
Cosing Volume = (G) x Volume in gal./11.= A/4 gals. 6.0 1.470
.-
Method of Wen Evacuation /If±:_ Start Time: //.4 TO CONVERT GAi/FT TO UTERS/FT, MULTIPLY ABOVE FIGURES BY
~,4{3 Time: / Z. .J ?f'
3.8 LITERS/GALLON. .·
Method of Sample Collection
Chain-of-Cusio<iy form Started {ryino)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 6th Volume
Volume Purged (gollons)
Time (mmtary)
.
pH {S.U.)
Sp. Cond. {umhos/cm)
Weter Te{llp. (•c) a
Odor (subjective)•
Turbidity (subjective)"
• (t)Hone (2)Slight (3)Moderale (4)Stronge
" (l)cleor (2)Slighfty Turbid (3)Moderotely Turbid (4)Very Turbid (5)Exlremely Turbid
Commenls/Observotions/Recommendolions; P-.::z. 2 . .JI. ,t,_L'"' <;...,-I
/ /
O& f form48 (3/94)
00014G
HNA Holdings, Inc.-Shelby, NC
Water-Level Measurements
Date: :--2&t! I Z I f '1"1'1
Measured by: #x: /pc1J,-rr
I
Page: l of
Mea~urement Device: ,.c-£.L!:.Cc'<--AI.""• =isur-c ____ _
Measuring Wetur
Monitor-Point Depth to Level Comments
Ing Elevetlon Water (fl) Elevation
Location (ft, mel) (ft, msl)
A-39 823.36 lb-~'I
B-34 790.62 :--IL~~----.-
C-49 864.1 I /J. 6l,
D-27 845.50 IX . .f 6
·D-35 845.69 /'J-Of,
D-56 845.19 /3. lb
D-88 845.52 IX. 9o
F-55 849.19 7£!, ,+
0-50 848.48 :;&. ,'l 1~
G-_88 848.26 7;& 3/"/j
H-59 845.25 4'J,,f0
H-79 846.53 Nf11 . /"/d-u.,, 7>rf:;5,t1,:,iJ4'1 -
1-57 837,63 J(,qif
J-29 825.18 1,,.0. l, /
J-59 825.01 1~1.e+
K-28 811.20 /'3.(Z--
K-58 811.39 IB 81
M-28 806.72 "70, -J j!..-;7):: 5/. 5'7
M-44 806.71 7P. 0,?
N-29 803.38 1''7 -et:;
N-53 803.82 /'7 ?1--
0-25 807.54 117•-'l 7
0-59 806.61 L-+ 03
P-31 790.00 2-;,. t&
P-58 788.12 ,z,f. I I
000147
Kubal-Furr & Associates
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Fax :[phone] uct 10 ""
HNA Holdings, lnc.-Shelby, NC
\Vater-LeYel Measurements
Date: ___________ _ Page:
I ,VV
of
Measured by: ________ _ Measurement Device: ________ _
Measuring
Monitor• Point
Ing Elevation
Location (It, msl}
Q-33 783.48
R-17 779.31
R-42 778.81
S-50 826.02
T-17 777.90
T-35 777.38
T-58 776.03
U-38 826.55
V•23 811.89
W-23 800.91 ._. ..
X-32 796.96
Y-38 794.52
y.74 794.87
Z.78 797.08
AA-41 783.68
AA-54 782.16
BB-18 771.75
CC-33 812.68
CC-64 811.37
DD-58 796.10
EE-58 794.48
FF-23 772.33
FF-34 772.73
FF-62 772.19
GG-25 771.64
Depth to I
Water
Level
Water (ft) Elevation
(ft, mal)
/Cf.~7 ' '
//./C.
/0, i,,(-i
J'J. 5 ;/,
I
1?,'fl ..
I/. '11-
'/,01
1-4711
14 10
11. z1-,
/(,, JI
/7-71
/1,,. 11 ...
·to, v 3/
'5&. )7
5f.01
5(, 1../
t-~ ?&
1qcr1
77f-31
~I'.:. S''5
In. 30
/,'l, 6 7
//. i/.s
AIM /J/,r!Nc-l,-,..
000148
Kubal-Furr & Associates
-
Comments
Oct 18 '98 l(:45
RNA Holdings, lnc.-Shelby, NC
\Vater-Level Measurements
Date: ___________ _ Page: of
r·. V4
Measured by: ________ _ Measurement Device: ________ _
Measuring Water -
Monitor-Point Depth to Leval
Ing Elevation Water (ft) Elevation
Comments
Location (ft, mel) (fl, msl)
GG-39 770.44 /7. bl
GG-61 771.78 Ix'.(.,'{ ..
HH-48 755.44 4-v.~v I
fill-77 755.87 [ .,,J,.,,. t q
PZ-1 773,99 fl,_. t3Cf
PZ-2 795,81 ½1'1
PZ-3 786.62 (Well Destroyed/Paved Over Between 8/95 and 11/95)
PZ-4 750.07
PZ-5A 788.72
Plr5B 777.59
PZ-6A 795.1 l
PZ-68 796.89
PZ-7A 780.46
PZ-7B 784.46
PZ-8 767.99
PZ-9 788.96
PZ-10 784.65
PZ-11 805.48
PZ-12 749.41
PZ-13 776.51
OT-lR 771.44
OT-2R 773.55
OT-3 792.88
OT-4 790.28
OT-5 784,00
,1, /7
J Z,, l-&
1-1-..-1 ·-
JI, i/o
'S'f. 'it
').;') -'JLf
r;,. '17..,
S". I(,,
i2..1q
7/, ti
,;,_, (:/I
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;2,/,'17 'V
S.c;'-1
s-'i'l
2 '(. r;;
·;.,1. J..7
'}_j.., '}.i
00014H
Kubal-Furr & Associates
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Water-LeYel Measurements
Date: ___________ _ Page: 4 of
Measured by: ________ _ Measurement Device: ________ _
Measuring Water -
Monitor-Point Depth to · Level Comments
Ing Elevation Water (ft) Elevation
Location (ft, msl) (ft, msl)
GT-6 787.45 1, I. 51
OT-6A 798.68 J'f. o(;,
--·---
OT-7 782.16 J0,06
OT-7A 782.52 I>• ol,
OT-8 782.26 Jo. g7
OT-IU 804.08 J.t/. 'i'i
IT-I 814.20 >109?
IT-2 813.85 t?1.7ltf
IT-3 809.66 1 z,J. ·Jo
IT-4 809.08 7;✓/ zl
IT-5 810.64 "JI '7 I
!T-6 812.20 11-, &t-
IT-7 813.52 vi Jo
IT-8R 813.04 Altt7
IT-9 808.73 /1111
PEW-I 846.85 f.,/q(;/
PEW-2 848.92 . -~ V (Well abandoned on 9/12/96)
PEW-3 849.25 771"71 --
PEW-4 848.14 --7,/ e1
TD-I /"7. Of..,
TD-2 ~&W
TD-3 ·7 2 r.,/
TD-4 ½.'.,o
T-1 lf,.~q
T-2 //.: lYJ
000150
Kubal-Furr & Associates
KUBAL-FURR~ H~~UL l..'1--,. ,. '-' _,.._,
HNA Holdings, lnc.-Shelby, NC
\Vater•Level Measurements
Date: ___________ _ Page: s of
Measured by: _________ _ Me,asurement Device: ________ _
Monitor-MeaRurlng
Point Ing Elevation
Location (ft, mlll)
Tl-I
11-2
S-1
Water
· Depth to Level
Water (ft) Elevation
(ft, msl)
?i ,.f.
·-:;f 7; t-
Z,l• ?l, I
OOOJ.51
Kubal-Furr & Associates
-
Comments
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Df\YIS
FLtJ\'D LABORATORY ANALYSIS REPORT
March 15, 1999
JERRY MCMURRAY
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
Login Number
Project Number
Description
:L99030213
:60885.00
: WASTEWATER
Dear Jerry Mcmurray:
We are pleased to provide the enclosed analytical results for the samples received by
Davis & Floyd, Inc. on March 02, 1999.
A formal Quality Assurance/Quality Control program is maintained by Davis & Floyd,
which is designed to meet or exceed the EPA or appropriate regulatory requirements.
All analytical analyses for this project met QA/QC criteria unless otherwise stated in the
footnotes. This report is to be reproduced only in full.
Feel free to contact our Client Services Representative at [phone] if further
explanation of the analysis is required. Unless other arrangements have been made, samples
will be disposed of or returned f4 days from the date of the report. We appreciate the
opportunity to provide services to your firm.
Sincerely, ·
DAVIS & FLOYD NC.//
/Y~~
n H. McCord, Jr
boratory Manager
0()0001
Davis & Floyd, Inc. l PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 2964•9 I (864) 229:7413 I Fax (864) ·229-7119
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
client
Contact
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITEF
Matrix
Parameter
Gas Chro~atography
SW846 8015
ETHYLENE GLYCOL
WW/STW/SFW
NC Certification Number: 25
Project Number: 60885.00
Report Date
Page 1 of 1
Sample ID
: March 15, 1999
L990302l3-0l
Date Collected: 02-MAR-99 13:54
Date Received: 02-MAR-99
Result Qual RDL Onit• Analyst Date Time
< 7.0 7.0 mg/1 MAT 03/08/99 1108
000002
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 \ 816 E. Durst Avenue \ Greenwood, SC 29649 ::------
1864) 229-4413 I Fax (864) 229,7119
Df\VIS
FLOYD LABORATORY ANALYSIS REPORT
client
Contact
HNA HOLDINGS INC,
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID: ITIF
Matrix
Parameter
aaa Chromatography
Sk'846 8015
ETHYLENE GLYCOL
WW/STW/SFW
NC Certification Number: 25
665
000003
Project Number: 60885.00
Report Date
Page 1 of 1
Sample ID
March 15, 1999
L99030213-02
Date Collected: 02-MAR-99 14:00
Date Received: 02-MAR-99
RDL Onita Analyat Date
140 mg/1 MAT OJ/08/99 1248
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 .,-:;-.... _
[phone] I Fax [phone]
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DAYIS
FLMD LABORATORY ANALYSIS REPORT
Master Tracking List
client
Contact
Sample ID
L99030213-01
Ga• Chromatography
SW846 8015
Gae Chromatography
SW846 8015
HNA HOLDINGS INC.
P.O. BOX 87
SHELBY, NC 28150
JERRY MCMURRAY
Client ID
ITEF
ITIF
NC Certification Number: 25
Project Number: 60885.00
Report Date
Page 1 of 1
March 15, 1999
Date Collected
02-MAR•99 13:03 02-MAR-99
03/08/99 1108
14,:03
OJ/08/99 1248
000004
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue ! Greenwood, SC 29649 I (864)229~413 I Fax [phone]
D1\VIS
FLtiYD LABORATORY ANALYSIS REPORT
Method Conformance Summary
Client: HNA HOLDINGS, INC.
Login: L990302l3
Semi
Criteria Volatiles Volatiles Metals
Sample Holding Time
Standards Preparation
Instrument Tuning
Instrument Calibration
Calibration Verification
Degradation Check
Interference
Sample/Standard
Blanks Results
Method Accuracy
Method Precision
Surrogate Recovery
PDSISD/MSA
TCLP Preparation
Key ✓
N/A
= Met Criteria Met
= Not Applicable
N/A N/A N/A
N/A N/A NIA
N/A N/A NIA
NIA N/A NIA
N/A N/A N/A
NIA N/A NIA
NIA NIA NIA
NIA NIA NIA
NIA N/A N/A
NIA NIA N/A
N/A NIA N/A
N/A N/A N/A
N/A NIA N/A
•
PDS =
SD =
MSA=
Method Criteria Not Met -See footnote(s) below .
Post Digestion Spike
Serial Dilution
Method of Standard Additions
Footnotes: Ethylene glycol summarized under column headed "Other".
Preparedby~Ll~
000()05
Project Number: 60885.00
Report Date: March 15, 1999
Inorganics Other
N/A ✓
N/A ✓
NIA NIA
NIA ✓
NIA ✓
NIA NIA
NIA NIA
NIA ✓
N/A ✓
N/A ✓
NIA NIA
N/A N/A
N/A NIA
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 296";9 I (864) 229r4413 I Fax [phone]
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D1\VIS
FLOYD
Method Blanks
Blank
Parameter
Ga• Chromatography
SW846 8015
ETHYLENE GLYCOL
MBl656l:l
LABORATORY ANALYSIS REPORT
Report Date ' March 1s, 1999
Page 1 of 1
Matrix WW/STW/SFW
WorkGroup: WG16561
Cone Qual RDL Units Analyst Date Tb1e
7.0 7.0 mg/1 MAT 03/08/99 1043
Davis & Floyd, Inc. \ PO Drawer 428 l Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Laborato,y Control Standards and Duplicates
LCS : LCS16561: l
STHYLENB GLYCOL 50.00 43.20
Report Date : March 15, 1999
Page 1 of 1
Matrix : WW/STW/SFW
WorkGroup: WG16561
Method : SW846 8015
80,l 70-130
000007
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue [ Greenwood, SC 29649 I (864) 229:;413 I Fax [phone]-
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DAYIS
FLtrYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
BTHYLENE GLYCOL
{\/;~:£:i:~~r. · · ·
ETHYLENE GLYCOL
MS/MSD MS99030213-0l:16561
MSD9903D213-0l:16561
50.00
50.00
<: 7.00
46. 20
Report Date
Page 1 of 1
March 15, 1999
Matrix WW/STW/SFW
WorkGroup: WG16561
Method SWB46 8015
50.01 106.9 41-152
91. 3 9.17 31 41-152
ononos
Davis & Floyd, Inc. I PO Drawer 428 \ Greenwood, SC 29648 ! 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229=i"413 \ Fax [phone]
-------· -Ch -·n f C -t d -R: -d -11111 lll'-Uf-a1 0 us 0 y ecor
,~-..... ,w .... ; ~ita Location a1e E. Our.tAvenue, Greenwood, SC 29649 (864) 229-+413 Fax:. [phone]
1,1,1 AIA' 4, J ,,.I, ,., ",, ,, ~ C)4::>-?-<70 j-Je/j._, Laboraftl,y Certlfr;ation Numbers: SC· 24110, NC. 25, TN-2923, VA-71
,----· / Report 10 , ..,opy To Reporting Requuement3.: t ) standard / J Data ~ackar,e (Specify LeveO
1 ....... i.ct.d uy
11 (' AJ_a-
R red Parameters, C<intainer.s and Preservatives
J,,/, r-
l ~ \I
NOTICE: ! ~
"' C \i .s ~ s r:; • t ...,_
0 ~ \\ 11 " " "'\ l I ~ J,
Samole Collectlon !. ! j ~ ~~
Samole Desaiotion Date Time Time ,vpe 1otal "
rr$r 3-,?-'-c.. /Jf-'I t 5 I I
1T.I,e:-t I--/,:,,, ;. ,, I I
-
R/P~#~ / D,te """ ',f'(OHquJsh&d By 0.19 Tlmo Rellqulshed By Dote n,,,.
>--~,;,; I~ -..,--
'.,, D,te i,me ,..ecefwdBy o,te nme ..,f!IC8lved In Labola~By Date Tlmo
WJ ft--'fr). 'P..K;..; ',.!).. t/4 ,1,15
-••~n~
Matrtx Type Denn!Uons 1 -Of1nk.lng Weter 2 • Creen Weter 5 • Groundwater 7 • Soll/Sediment 8 • Liquid Sludge g • Oil 12-Alr
Preservative OeflnlUons A -None B -H2S0-4 C • HCI D. HN03 E • NaOH F -Filtered G • Other
----Page __ of __
ceuu
,....,, .... ,ase urder
Stata uU019
}J(__ /
Loam ISpoda/ Instructions ,
' ~ ' I !I t~ ~1 '
..J i
,,=on HOT ....ummenlS
{)/
O').
C ')
J
( 1
C::l -_,
(" ..,
uu"G) 1~h/0
y N """' """' If Y, spijcHy: Alrbl/1 Numbttr
_:=day11
Cooler ID ~able}:
On Ice: Yes/ o Temp(C) '!:::::::'
Custody Seal: Intact / Brok._,, 7, Non4 .I
Davts & r,aya, fnc.
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DAYIS
FLtrYD LABORATORY ANALYSIS REPORT
May 06, 1999
JERRY MCMURRAY
TICONA, LLC.
PO BOX 87
SHELBY, NC 2850
:L99041201
:60885.00-0002
Logii1 Number
Project Number
Description :GROUNDWATER SAMPLING & ANALYSIS
Dear Jerry Mcmurray:
We are pleased to provide the enclosed analytical results for the samples received by
Davis & Floyd, Inc. on April 09, 1999.
A formal Quality Assurance/Quality Control program is maintained by Davis & Floyd,
which is designed to meet or exceed the EPA or appropriate regulatory requirements.
All analytical analyses for this project met QA/QC criteria unless otherwise stated in the
footnotes. This report is to be reproduced only in full.
Feel free to contact our Client Services Representative at [phone] if further
explanation of the analysis is required. Unless other arrangements have been made, samples
will be disposed of or returned f4 days from the date of the report. We appreciate the
opportunity to provide services to your firm.
Sincerely,
DAVIS & FLOYD, NC.
rl~ (9:.i_ McCord, Jr
LAb~!:nory Manager
000001
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Client
Contact
TICONA, LLC.
PO BOX 87
SHELBY, NC 2850
JERRY MCMURRAY
client ID: ITCI
Matrix
Para.meter
aas Chromatography
SW846 8015
ETHYLENE GLYCOL
Volatile Organics
: GW/ChemW
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROBTHANE
1,1,2-TRICHLOROETHANB
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONB
ACETONE
BENZENE
BROMODICHLOROMETHANB
BROMOFORM
BROMOMETH.ANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TBTRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENB
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
<
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SC Certification Number: 24110
Project Number: 60885.00-0002
Report Date ' May 06, 1999
Page 1 of 2
Sample ID L99041201-0l
Date Collected: 09-APR-99 11 : 25
Date Received ' 09-APR-99
Re■ult RDL Onita Analyst Date Timo
1510 70.0 mg/1 MAT 04/13/99 1211
0.020 X 0.020 mg/1 PAP 04/16/99 1807
0.020 X 0.020 mg/1 PAP 04/16/99 1807
0.020 X 0. 020 mg/1 PAP 04/16/99 1807
0.020 X 0.020 mg/1 PAP 04/16/99 1807
0.020 X 0. 020 mg/1 PAP 04/16/99 1807
0.020 X 0. 020 mg/1 PAP 04/16/99 1807
0.020 X 0.020 mg/1 PAP 04/16/99 1807
0.041 0.040 mg/1 PAP 04/16/99 1807
0.040 X 0 .040 mg/1 PAP 04/16/99 1807
0.020 X 0 .020 mg/1 PAP 04/16/99 1807
0.84 0. 040 mg/1 PAP 04/16/99 1807
0.027 0.020 mg/1 PAP 04/16/99 1807
0. 020 X 0.020 mg/1 PAP 04/16/99 1807
0. 020 X 0.020 mg/1 PAP .04/16/99 1807
0.040 X 0 . 040 mg/1 PAP 0_4/16/99 1807
0.020 X 0.020 mg/1 PAP 04/16/99 1807
0.020 X 0.020 mg/1 PAP 04/16/99 1807
0. 020 X 0.020 mg/1 PAP 04/16/99 1807
0.040 X 0.040 mg/1 PAP 04/16/99 1807
0. 020 X 0 . 020 mg/1 PAP 04/16/99 1807
0.040 X 0.040 mg/1 PAP 04/16/99 1807
0.020 X 0.020. mg/1 PAP 04/16/99 1807
0.020 X 0 .020 mg/1 PAP 04/16/99 1807
0.020 X 0.020 mg/1 PAP 04/16/99 1807
0.020 X 0.020 mg/1 PAP 04/16/99 1807
0.020 X 0.020 mg/1 PAP 04/16/99 1807
0. 020 X 0. 020 mg/1 PAP 04/16/99 1807
0.020 X 0.020 mg/1 PAP 04/16/99 1807
0.020 X 0.020 mg/1 PAP 04/16/99 1807
0.020 X 0.020 mg/1 PAP 04/16/99 1807
0.020 X 0. 020 mg/1 PAP 04/16/99 1807
0. 020 X 0.020 mg/1 PAP 04/16/99 1807
0.040 X 0.040 mg/1 PAP 04/16/99 1807
0.040 X 0.040 mg/1 PAP 04/16/99 1807
0.020 X 0. 020 mg/1 PAP 04/16/99 1807
000002
Davis & Floyd, Inc. 1 PO Drawer 428 ! Greenwood, SC 29648 I 816 E. Ours! Avenue I Greenwood, SC 29649 I [phone] I Fax {864) 229-7119
Df\YIS
FLffi'D
Client
Contact
TICONA, LLC.
PO BOX 87
SHELBY, NC 2850
JERRY MCMURRAY
client ID: ITCI
Parameter
Wet Chemistry
SW846 9060
ORGANIC CARBON, TOTAL
LABORATORY ANALYSIS REPORT
SC Certification Number: 241 JO
Project Number: 60885.00-0002
Report Date
Page 2 of 2
May 06, 1999
Sample ID L99041201-0l
Reault Qual RDL Unit• Analyst Date
2530 10.0 mg/1 TRB 04/15/99 0955
000003
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
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Di\YIS
FLOYD
Client
Contact
TICONA, LLC.
PO BOX 87
SHELBY, NC 2850
JERRY MCMURRAY
client ID: ITEF
Matrix
Parameter
Gas Chromatography
SW846 8015
ETHYLENE GLYCOL
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-0ICHLOROETHANE
1,2-DICHLOROPROPANE
2-Btrr.ANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
GW/ChemW
LABORATORY ANALYSIS REPORT
<
<
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SC Certification Number: 24110
Re11ult
Project Number: 60885.00-0002
Report Date
Page 1 of 2
Sample ID
: May 06, 1999
L99041201-02
Date Collected: 09-APR-99 11:40
Date Received: 09-APR-99
RDL Unit• Analyst Date Time
7.0 7.0 MAT 04/13/99 1004
0.0050 0.0050 mg/1 PAP 04/16/99 1130
0.0050 0.0050 mg/1 PAP 04/16/99 1130
0.0050 0.0050 mg/1 PAP 04/16/99 1130
0.0050 0.0050 mg/1 PAP 04/16/99 1130
0,0050 0.0050 mg/1 PAP 04/16/99 1130
0.0050 0.0050 mg/1 PAP 04/16/99 1130
0.0050 0.0050 mg/1 PAP 04/16/99 1130
0.010 0.010 mg/1 PAP 04/16/99 1130
0.010 0.010 mg/1 PAP 04/16/99 1130
0.0050 0.0050 mg/1 PAP 04/16/99 1130
0. 010 0.010 mg/1 PAP 04/16/99 1130
0.0050 0.0050 mg/1 PAP 04/16/93 1130
0.0050 0.0050 mg/1 PAP 04./16/93 1130
0,0050 0.0050 mg/1 PAP _04./16/99 1130
0. 010 0. 010 mg/1 PAP 0_4./16/99 1130
0.0050 0.0050 mg/1 PAP 04/16/99 1130
0.0050 0.0050 mg/1 PAP 04/16/99 1130
0.0050 0.0050 mg/1 PAP 04/16/99 1130
0. 010 0. 010 mg/1 PAP 04/16/99 1130
0.0050 0.0050 mg/1 PAP 04./16/99 1130
0.010 0.010 mg/1 PAP 04/16/99 1130
0.0050 0.0050 mg/1 PAP 04/16/99 113 0
0.0050 0.0050 mg/1 PAP 04/16/99 1130
0.0050 0.0050 mg/1 PAP 04./16/99 1130
0.0050 0.0050 mg/1 PAP 04/16/99 1130
0.0050 0.0050 mg/1 PAP 04/16/99 1130
0.0050 0.0050 mg/1 PAP 04/16/99 1130
0.0050 0.0050 mg/1 PAP 04/16/99 1130
0.0050 0.0050 mg/1 PAP 04./16/99 1130
0.0050 0.0050 mg/1 PAP 04./16/99 1130
0,0050 0.0050 mg/1 PAP 04/16/99 1130
0.0050 0.0050 mg/1 PAP 04/16/99 1130
0.010 0.010 mg/1 PAP 04./16/99 1130
0.010 0.010 mg/1 PAP 04/16/99 1130
0.0050 0.0050 mg/1 PAP 04/16/99 1130
000004
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 1 816 E. Durst Avenue I Greenwood, SC 29649 ] [phone] I Fax [phone]
Di\YIS
FLOYD
Client
Contact
TICONA, LLC.
PO BOX 87
SHELBY, NC 2850
JERRY MCMURRAY
Client ID: ITEF
Parameter
Wet Cbami11try
SW846 9060
ORGANIC CARBON, TOTAL
LABORATORY ANALYSIS REPORT
SC Certification Number: 241 JO
Project Number: 60885.00-0002
Report Date
Page 2 of 2
May 06, 1999
Sample ID L99041201-02
R••ult Qual RDL units Analyst Date TilH
12.7 1.0 mg/1 TRB 04/15/99 1042
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000005
Dav;s & Floyd, Inc. I PO D,awer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone] I
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DAYIS
FLOYD
Client
Contact
TICONA, LLC.
PO BOX 87
SHELBY, NC 2B50
JERRY MCMURRAY
Client IO: ITEF DOP.
Matrix
Par.meter
aa■ chromatography
SWB46 B015
ETHYLENE GLYCOL
Volatile Organica
SWB46 8260B
l,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
C!S-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
GW/ChemW
LABORATORY ANALYSIS REPORT
SC Certification Number: 24110
Reault
< 7.0
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0. 010
< 0.010
< 0.0050
< 0.010
< 0.0050
< 0.0050
< 0.0050
< 0.010
< 0.0050
< 0.0050
< 0.0050
< 0.010
< 0.0050
< 0.010
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.0050
< 0.010
< 0.010
< 0.0050
000006
Project Number: 60885.00-0002
Report Date
Pagel of 2
Sample ID
: May 06, 1999
Date Collected: 09-APR-99 11:40
Date Received : 09-APR-99
RDL Onita Analyst Date Time
7.0 mg/1 MAT 04/13/99 1119
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.010 mg/1 PAP 04/16/99 1149
0.010 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.010 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP . 04/16/99 1149
0. 010 mg/1 PAP ~4/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.010 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.010 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
0.010 mg/1 PAP 04/16/99 1149
0.010 mg/1 PAP 04/16/99 1149
0.0050 mg/1 PAP 04/16/99 1149
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229-441 3 I Fax [phone]
Di\YIS
FLOYD
Client
Contact
TICONA, LLC,
PO BOX 87
SHELBY, NC 2850
JERRY MCMURRAY
Client ID: ITEF DUP,
Wet Chami•try
SWB46 9060
ORGANIC CARBON, TOTAL
LABORATORY ANALYSIS REPORT
SC Certification Number: 24110
Project Number: 60885.00-0002
Report Date
Page 2 of 2
May 06, 19!:19
Sample ID L99041201-03
Re■ult Qual RDL Unite .Analy•t Date Time
••• 1. a mg/1 TRB 04/15/99 1110
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Davis & Floyd. Inc. I PO 0,awer 428 I Greenwood. SC 2%48 I 81~EQD~s~~n:. I Greenwood. SC 2%49 I [phone] I Fax [phone]
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DAYIS
FLOYD
Client
Contact
TICONA, LLC.
PO BOX 87
SHELBY, NC 2B50
JERRY MCMURRAY
Client ID: K-28
Parameter
Field Data
EPA 170.l
TEMPERATURE:
SW846 9040B
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Wet Chemistry
SWB46 9060
ORGANIC CARBON, TOTAL
GW/ChemW
LABORATORY ANALYSIS REPORT
SC Certification Number: 24110
18.0
6.7
330
795.79
43.0
Project Number: 60885.00-0002
Report Date
Page 1 of 1
Sample ID
May 06, 1999
L99041201-04
Date Collected: 09-APR-99 13:06
Date Received
Qual RDL Units Analy•t Date Tim•
1.0 degreeo C 04/09/'J9 1306
0.50 GU 04/09/99 1306
1.0 umhoa/cm 04/09/99 1306
.01 feet MSL 04/09/99 1306
1.0 mg/1 TRB 04/15/99 1125
000008
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 1 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAJ'IS
FLtJ\'D
Client
Contact
TICONA, LLC.
PO BOX 87
SHELBY, NC 2850
JERRY MCMURRAY
Client IO: V-23
Par-.w.eter
Field Data
EPA 170.l
TEMPERATURE
SWB46 904GB
PH
SW846 9050
Matrix
SPECIFIC CONDUCTIVITY
GROUND WATER ELEVATION
Wet Cheril.istry
SWB46 9060
ORGANIC CARBON, TOTAL
GW/chemW
LABORATORY ANALYSIS REPORT
SC Certification Number: 24110
Project Number: 60885.00-0002
Report Date May 06, 1999
Page l of 1
Sample ID L9904120l-OS
Date Collected: 09-APR-99 13:36
Date Received ' 09-APR-99
Re11ult Qual RDL Onita Analy■

t

Oat• Time
17. 0 1.0 degrees C 04/09/99 1336
5.1 0.50 OU 04/09/99 1336
5570 1. 0 umhos/cm 04/09/99 1336
. 01 feet MSL 04/09/99 1306
7760 10.0 mg/1 TRB 04/15/99 1153
000009
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (8641 229-4413 I Fax [phone] I
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FLtrYD
Client
Contact
TICONA, LLC.
PO BOX 87
SHELBY, NC 2850
JERRY MCMURRAY
client ID: TRIP BLANK
Matrix
Para.m•t•r
Volatile Organics
SW846 B260B
1,1,l·TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2-HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-l,2-01CHLOROETHEN6
CIS-l,3-DICHLOROPROP6N6
DIBROMOCHLOROM6THAN6
6THYLB6NZ6NE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROBTH6N6
TRANS-1,3-DICHLOROPROPENE
TRICHLOR06THEN6
VINYL ACSTATE
VINYL CHLORIDE
XYLENE (TOTAL)
GW/ChemW
LABORATORY ANALYSIS REPORT
<
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<
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SC Certification Number: 24110
Result
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.010
0.010
0.0050
0. 010
0.0050
0.0050
0.0050
0.010
0.0050
0.0050
0.0050
0.010
0.0050
0.010
0.0050
0.0050
o. 0050
0 .0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.010
0.010
0.0050
Project Number: 60885.00-00D2
Report Date
Page 1 of 1
Sample ID
: May 06, 1999
L99041201-06
Date Collected: 08-APR-99 08:00
Date Received: 09-APR-99
RDL
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
D. 0050 mg/1 PAP
0. 0050 mg/1 PAP
0.010 mg/1 PAP
0.010 mg/1 PAP
0.0050 mg/1 PAP
0.010 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.010 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.010 mg/1 PAP
0.0050 mg/1 PAP
0.010 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0.0050 mg/1 PAP
0. 010 mg/1 PAP
0.010 mg/1 PAP
0.0050 mg/1 PAP
000010
04/16/'H
04/16/99
04/16/99
04/16/99
04/16/99
04/16/99
04/16/99
04/16/99
04/16/99
04/16/99
04/16/99
04/16/99
04/16/99
04/16/99
04/16/99
04/16/99
04/16/99
.04/16/99
04/16/99
04./16/99
04/16/99
04/16/99
04./16/99
04./16/99
04./16/99
04./16/99
04./16/99
04./16/99
04./16/99
04/16/99
04/16/99
04/16/99
04./16/99
04./16/99
04./16/99
Time
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
1112
Davis & Floyd, Inc. ] PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLtfYD LABORATORY ANALYSIS REPORT
SC Certification Number: 24110
Master Tracking List
Client
Contact
Sam.pl• ID
Oas Chromatography
SW846 8015
Volatile Organics
SWB46 8260B
Wet Chemistry
SW846 9060
L99041201-0l
Oas Chromatography
SW846 8015
Volatile organics
SW846 8260B
Wat Chomi■try
SW846 9060
L99041201-03
Oaa Chromatography
SW846 8015
Volatile Organic■
St-.'846 8260B
Wat Chemistry
SW846 9060
L99041201-04
Field Data
EPA 170.l
SWB46 9040B
SW846 9050
TICONA, LLC.
PO BOX 87
SHELBY, NC 2850
JERRY MCMURRAY
Client ID
ITCI
ITEF
ITEP' DO'P.
K-28
Project Number: 60885.00-0002
Report Date
Page 1 of 2
May 06, 1999
11:04
09-APR-99 11:04
09-APR-99 11:04
09-APR-99 13:04
04/13/99 1211
04/16/99 1807
04/15/99 0955
04/13/99 1004
04/16/99 1130
04/15/99 1042
09-APR-99
04/13/99 1119
04/H/99 1149
04/15/99 1110
04/09/99 1306
04/09/99 1306
04/09/99 1306
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000011
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I 1864) 229-4413 I Fax [phone] I
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Df\VIS
FLOYD LABORATORY ANALYSIS REPORT
Master Tracking List
Sample ID
Wet Chemistry
SW846 9060
L9904l201-05
Field Data
EPA 170.1
SW846 9040B
SW846 9050
Wet chemistry
~ SW846 9060
L!Hl041201-06
client
Contact
Volatile Organics
SW846 8260B
TICONA, LLC.
PO BOX 87
SHELBY, NC 2850
JERRY MCMURRAY
client ID
V-23
TRIP BLANK
SC Certification Number: 24110
Project Number: 60885.00-0002
Report Date May 06, 1999
Page 2 of 2
Date Collected Date Received
04/15/99 1125
09-APR-H 13:04 09-APR-99
04/09/99 1336
04/09/99 1336
04/09/99 1336
04/15/99 1153
08:04
04/16/9'J 1112
000012
Davis & Floyd, Inc. 1 PO Drawer 428 \ Greenwood, SC 29648 l 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax {864) 229-7119
Df\YIS
FLOYD LABORATORY ANALYSIS REPORT
Method Conformance Summary
Client: HNA HOLDINGS, INC.
Login: L9904l20I
Criteria Volatiles
Sample Holding Time
Standards Preparation
Instrument Tuning
Instrument Calibration
Calibration Verification
Degradation Check
Interference
Sample/Standard
Blanks Results
Method Accuracy
Method Precision
Surrogate Recovery
PDS/SD/MSA
TCLP Preparation
Key ✓
NIA
= Met Criteria Met
= Not Applicable
✓
✓
✓
✓
✓
NIA
NIA
✓
•
✓
✓
NIA
NIA
Semi
Volatiles
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
Metals
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
NIA
• Method Criteria Not Met -See footnote(s) below .
Post Digestion Spike ' PDS =
SD =
MSA=
Serial Dilution
Method of Standard Additions
Footnotes: TOC is summarized under "Inorganics" column.
Ethylene glycol is summarized under "Other" column.
Project Number: 60885.00-0002
Report Date: May 3, 1999
Inorganics Other
" " " " NIA NIA
" " " " NIA NIA
NIA NIA
" ✓
✓ ✓
✓ ✓
NIA NIA
NIA NIA
NIA NIA
"Spike Added" amounts are given in ug/L on Volatile "Matrix Spikes and
Duplicates" and "Laboratory Control Standard and Duplicates" summaries.
"Spike Added" amounts are given in mg/Lon Ethylene Glycol and Total Organic
Carbon "Matrix Spikes and Duplicates" and "Laboratory Control Standard and
Duplicates" summaries.
Toluene recovered at 82.8% and 89.8% in the MS and MSD respectively. The lower
control limit for toluene is 84%.
PreparedbcY~l ~~
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Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 ~ D~r?A?.n~e ~ Greenwood, SC 29649 I (8641 229-4413 I fax [phone] I
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DAYIS
FLMD
Method Blanks
Blank : MB170S3:l
Parameter
Volatile Organics
SW846 8260B
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-0ICHLOROETHANE
1,1-0ICHLOROETHENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
2-BUTANONE
2 -HEXANONE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
ETHYLBENZENE
METHYLENE CHLORIDE
STYRENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-0ICHLOROETHENB
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
VINYL ACETATE
VINYL CHLORIDE
XYLENE (TOTAL)
LABORATORY ANALYSIS REPORT
Report Date May 04, 1.999
Page 1 of 1
Matrix GW/ChemW
WorkGroup: WG17053
Cone Qual RDL Unite Analyst Dat• Time
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5. 0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 10.0 10.0 ug/1 PAP 04/16/99 0832
< 10.0 10.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 10.0 10.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 10.0 10.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 10.0 10.0 ug/1 PAP 04/16/99 0832
< 5.0 5 .0 ug/1 PAP 04/16/99 0832
< 10.0 10. 0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 5.0 5.0 ug/1 PAP 04/16/99 0832
< 10.0 10.0 ug/1 PAP 04./16/99 0832
< 10.0 10.0 ug/1 PAP 04./1.6/99 0832
< 5.0 5.0 ug/1 PAP 04./16/99 0832
000014
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
1,1-0ICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
MS99041412-0l:l7053
MSD99041412-0l:l7053
50.00
50. 00
so. 00
50.00
50.00
50.00
50.00
50.00
so.co
so.co
< 5.00
< 5.00
< s.oo
< 5.00
< 5.00
41. 78
41.49
46 .13
44,91
47. 74
Report Date
Page 1 of l
May 04, 19Sl9
Matrix GW/ChemW
WorkGroup: WG17053
Method SW846 82608
45. 26
52.00
48. 48
41. 42
49.48
83.6
83.0
92 .3
89.8
95.S
90.S
104.0
97.0
82.8
9!¼. 0
6,62
11.2
0. 454
21.7
14.2
74-125
83-123
82-120
84-120
83-123
12
10
12
10
11
74-125
83-123
82-120
84-120
83-123
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000015
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Ours! Avenue I G,eenwood, SC 29649 I 18641 229-4413 I Fax [phone]
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Laborat01y Control Standards and Duplicates
LCS
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
LCS17053:l
20.00
20.00
20.00
20.00
20.00
17.23
19.33
19.31
19. 56
19. 28
Report Date
Page 1 of 1
May 04, 1999
Matrix· GW/ChemW
WorkGroup: WG17053
Method
86.2
96.7
96.6
97.8
96. 4
SW846 8260B
70-126
85-121
82-119
83-122
81-122
000016
Davis & Floyd, Inc. I PO Drawer 428 \ Greenwood, SC 29648 I 816 E. Durst Avenue l Greenwood, SC 29649 I [phone] I Fax [phone]
D1\VIS
FLOYD LABORATORY ANALYSIS REPORT
Surrogates % Recovery
Measureoate··
L99041201-0l 16-APR-99 18:07
L99041201-02 16-APR-99 11: 30
L99041201-03 16-APR-99 11: 49
L99041201-D6 16-APR-99 11: 12
LCS170S3:1 16-APR-99 13 : 4 8
MB17053:1 16-APR-99 08: 3 2
MS99041412-0l: 17053 16-APR-99 l O: 52
MS099041412-91:l7053 16-APR-99 10: 13
DCB 1,2-DICHLOROETHANS-D4
BFB BROMOFLUOROBENZENE
TOL TOLUENE-DB
116. 5 102. 5
91.5 88.2
90.9 89.6
94.2 86.9
112. 8 97.1
108.1 96.5
85,4 92.1
101.7 89.4
Report Date
Page 1 of l
Matrix
Method
103.1
100.5
102.0
98.8
102.6
103,0
106.2
98.8
May 04, 1999
GW/ChemW
SW846 8260
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000017
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue l Greenwood, SC 29649 I (864) n9-4413 I Fax [phone]
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Di\YIS
FLOYD
Method Blanks
Blank
Parameter
Gas Chromatography
Sk'846 8015
ETHYLENE GLYCOL
: MB17061:l
LABORATORY ANALYSIS REPORT
Report Date ' May 04, B99
Page 1 of 1
Matrix GW/Chemw
WorkGroup: WG17061
Cone Qual RDL Units Analyst Date Tim•
< 7.0 7.0 mg/1 MAT 04/13/99 0940
000018
Davis & Floyd, Inc. \ PO Drawer 428 I Greenwood, SC 29648 1 816 E. Durst Avenue I Greenwood, SC 29649 I [phone] j Fax [phone]
Df\YIS
FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
BTHYLBNB GLYCOL
MS99041201-02:17061
MSD99041201-02:17061
Report Date
Page 1 of l
Matrix
May 04, 1999
GW/ChemW
WorkGroup: WG17061
Method SW846 8015
· ·. ::--?/iPLkt\ :::::<:;::/s_atnp~e:-:·-::r/Mg::p · -.-.. .-,-::-::-:·-,Ms:-.. ···· :\::.:_:_ Liiliit;f.
''::."A~~-~d)\:':':"· -_:-~g~=ci\ :=t.-.:::/\}~ri;;f,: ??)}\'Ri8/:/' -·:::=:.::-::_~R~;/ ·_:":-.
50.00 <: 7.00 50.41 98,8 65-144
Li\1\:i."t:."s::°:"· \R~J,-: ·.-;R~c/>:.::-,'
50.00 49.14 100.2 0.585 21 65-144
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Dav;, & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. D~rs~~n~ ~ ;reenwood, SC 29649 I 1864) 229-441 J I Fax [phone] I
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DAYIS
FLt1YD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
··:':.~ara~(!~-~-r
ETHYLENE GLYCOL
LCS : LCS17061:l
so.co
Report Date May 04, 1999
Page 1 of l
Matrix GW/ChemW
WorkGroup: WG17061
Met.hod SW846 8015
/::"L."ifui t~·:./:/-_.:,
/t~~-i~·-,;_q)t
39.53 75.0 59-139
000020
Davis & Floyd, Inc. 1 PO Orav .. 'er 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 ] {864) 229-4413 I Fax {864) 229-7119
DAYIS
FLMD
Method Blanks
Parameter
Wet Chemistry
SW846 9060
Blank
ORGANIC CARBON, TOTAL
MB17088:l
LABORATORY ANALYSIS REPORT
Report Date
Page 1 of 1
May 04, 1999
Matrix GW/ChemW
WorkGroup: WG17088
Cone Qual RDL Units Analyat Dat• Tim•
1.0 1. 0 mg/1 TRB 04/15/99 1435
00002:t
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Davis & Floyd, lnc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue I Greenwood, SC 29649 I (864) 229,4413 I Fax [phone]
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DAYIS
FLOYD LABORATORY ANALYSIS REPORT
Matrix Spikes and Duplicates
MS/MSD
ORGANIC CARBON, TOTAL
ORGANIC CARBON, TOTAL
MS990412Dl-03:17088
MSD99041201-03:17088
20.00
20.00
Report Date May 04, 1999
Page 1 of 1
Matrix GW/ChemW
WorkGroup: WG17088
Method SW846 9060
8.75 30.70 109.8 74-132
29,50 103.8 3.99 11 74-132
00002'.1
Davis & Floyd, Inc. I PO Drawer 428 I Greenwood, SC 29648 I 816 E. Durst Avenue ! Greenwood, SC 29649 I [phone] I Fax [phone]
DAYIS
FLtiYD LABORATORY ANALYSIS REPORT
Laboratory Control Standards and Duplicates
LCS : LCS17088:1
ORGANIC CARBON, TOTAL 10.00 9.00
Report Date : May 04, 1999
Page 1 of 1
Matrix : GW/ChemW
WorkGroup: WG170BB
Method : SW846 9060
90.0 90-110
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Dav;s & Floyd, Inc. \ PO Dcawec 428 \ Gceenwood, SC 29648 \ 816 ~ ?u?. 2e:: \ Gceenwood, SC 2%49 \ (864) 229-441 3 \ fax [phone] I
- -- -- -- --------- - --DtcXJShf•"'·' lrmiltdlre FL YD inir"'"""1 Hm""1 -Chain of Custody Record Page __l_ of __i_
Client Project I Site Location 816 E. Durst Avenue, Greenwood, SC 29649 [phone] Fax: [phone]m1ce se umy
HNA Holdings 60885.00, Task 0002 Laboratory Certifcation Numbers: SC-24110, NC-25, TN· 2923, VA-77
Shelby, NC
Contact Report To Copy To Reporting Requirements: { J Standard [ J Data Package (Specify Level) Purchase Order
Jerry McMurray
Collected By Required Parameter.;, Containers and Preservatives State Quote
E ~i " NC
~~ r5-£:! E
J.G. Jenkins, Ill 0 LOQln Special Instructions v • N
NOTICE: ~ " a 2 <D -J!i • 0 I ~~ C :;: :~~ 12 0 •
C ~ 8 C e
'6 ~.
C C 0 ,_~ = 0 0 5 & C ,a ~-2 0 E~ :ll . " ~ :3 ·a • • "' u 0 X .• C -~ ~ • il" ~ D D { E :s E 0 0
Sample Collection E o 0 • • , e ~ 5 <;)-~ <ti ·-~ 0 ., " z w ...J
Samnle Descrintion Date Time Time Type Total B C A Fraction HOT Commems
Trip Blank Ii" qq ()f((Y) y le 7 L. 00
-TTr T IC 0(/ 117, 'f.. i:_ c; I 7 c 0/
C TTr.:P /II-IA X 5 c_ I 7 7 O'L
':::: ITT/7-" I\ r.L r~➔ e I IJ.J () V c:_ 5 I 7 7 01
k-7Q " 12/1 c... )( C I ol/ • • I -
~ 1/ . 7 .'<,. n-z,i;, X C I I fl5
Reliquished By i .~ 1,i1: te Time Reliquished By Date Time Reliquished By Date Time Quick[!!;, Shi~y
0 'l-'I I\ n ' Trr 1nn ,t:tJn y N ~, CllENT
""' FE()E;,,;
~eiveaBy CJ ' u te Time Received By Date Time ;;;;;_Lrn~a, tJ.V,~5
Date Time If Y, specify: Airbil/Number
1/-. o. /}/1 lft'/-D --days
_(.;omments
Cooler IGvailable):
On Ice: Ye / No Temp(C) _!I:'__
Custody Seal: Intact / Broken 1/4ione)
Matrix Type Deflnitions 1 -Drinking Water 2 -Clean Water 5 • Groundwater 7 -Soil/Sediment 8 -Liquid Sludge 9-0il 12-Air Davis & F/aya, -me.
Preservative Definitions A-None B -H2S04 C • HCI D • HN03 E -NaOH F -Filtered G -Other FL02_01 (02/P9)
ENGINEERS ARCHITECTS FIELD DAT A LOG Di\)/1S
FLOYD PLANNERS SCIENTISTS FOR GROUNDWATER SAMPLE COLLECTION/
CHARLESTON • GREENWOOD • COLUMBIA GROUNDWATER ELEVATION MEASUREMENTS :?'.?
Well No.: t-~
Client: _ __JW-/..lJ..,/''\----------------
Sile Name: S6,lb) ,
Dole: H·q.q9
Sampling Personnel:_~~~-----------
Site Personnel: ________________ _
Regulatory Personnel: ______________ _
Weather Condilions:_L\ /J~'~'L) 7+-______ Temp.: '6 ()
Well Oiomeler: ______ 1. __ · _O ___ ln.
(A) Top ol Well [levolion: ---~6~/L/ ~· _,'2_~0 __ msl (yes/no)
(B) Oeplh lo Immiscible Loyer.'------'~'-'l'-"A:'-'--f'-'I..
(C) Immiscible Loyer Elevolion: (A)-(B)=__,/\..u.cl A-!1..._ msl (yes/no)
(0) Depth to Groundwater. / f-'-j I fl.
(E) Groundwoler Elevation: (A)-(0)= 7 9 J::1 / C, msl (yes/no)
(F) Total Well Depth = _____ ..cl..__.,f'--.-'()"---------'f"I.
(G) Length of Waler Column: (F)-(D)= I 'Z., S-~ fl.
Cosing Volume = (G) x Volume in gol./ft.= l . / gals.
Method of Well Evacuation -=-"¼'----Siar! Time:/ LO(;,
Method of Sample Collection _l!.lL-'!;)/,L----Time: j 3Q(,
Chain-of-Custody Form Started
$ource(s) ol Well ID f"':90
Well Completion: Proleclive Cosing ~no)
10 Lobel (yes~
Flush (yes~)
Flush-Moun! Cover Seal lnlacl (yes/no) Locking Cop (yes/no)
Lacked al Arrival (~) Oeporlur~/no)
Well Cosing (heigh! abave/deplh below) ground: __ S::~--~U~-
Coslng Type ~ (Steel) (Other) ___________ _
Oedicoled Pump or Bailer Qno) Type U,Je Cl U Ii 2 iA
Protective Post/Ab~lmenl ~no) Concrete Pod {;)/no)
Well lnlegrily 5o 'sfoclor@no) If no. explain below.
moderole / high )
WELL VOLUME DATA
DIA. OF PIPE (in.) VOLUME IN GAL/Fl.
1.0
2.0
3.0
4.0
5.0
6.0
0.041
0.163
0.367
0.653
1.020
1.470
TO CONVERT GAL/f1 TO UTERS/f1, MULTIPLY ABOVE FIGURES BY
3.8 LITERS/GALLON.
FIELD ANALYSES
Volume Purged (gallons)
TTme (military)
pH (S.U.)
Sp. Cond. (umhos/ cm)
Water Temp. ("C)
Odor (subjective)•
Turbidity (subjective)"
1st Volume
• (t)None (2)Slighl (3)Moderole (4)Slrong
4th Volume 5th Volume
" (l)Cleor (2)Slightly Turbid (3)Moderolely Turbid (4)Very Turbid (S)Exlremely Turbid
Commenls/Observations/Recommendalions: ---------------------------
FORM COMPLETE:A~:: ~m)~J: I il[
D& F Form48 (3/94)
00002s
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I DAJ!IS
FLOYD
ENGINEERS
PLANNERS
ARCHITECTS
SCIENTISTS
FIELD DATA LOG
FOR GROUNDWATER SAMPLE COLLECTION/
GROUNDWATER ELEVATION MEASUREMENTS
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ARLESTON • GREENWOOD • COLUMBIA Well No · V · 7_) ..
H II tJ_ ' mo e2 10 label l];;/na) Client: Source{s) of Well ID
Site Name: ) LI h1 1 A.,[, Job Ho.:wi<M.(l) ,~,k QOL Well Completion: Prolecfive Cosing cfJ;,> flush {yes/€)
'
Dale: f g-~~ LWR submilled by: ~/A, flush-Mount Cover Seal Intact (yes/no) Locking Cap (yes/ no)
Sampling Personnel: :::s:cce locked at Arrival E}o) Departure (J;/no)
Site Personnel: -Well Casing {~depth below) ground: Z..-) ft.
Regulatory Personnel: -Casing Type {PVC) (Steel) (Other)
Weather Conditions: I 1/1~11 Temp.: yr) Dedicafed Pump or Bailer Cres/no) Type llte u IJ. r,;uJ
--~ u
Well Oiameler: 7..-, 0 In. Protective Post/Abulmenl (vesfno Concrete Pad (~)
~ll-'61 T
(A) Top of Well Elevation: msl (yes/no) Well Integrity Salisfo~ no) If no, explain below.
(B) Depth to Immiscible layer: '1J A; ft. Well Yield ( low / odera / high )
(C) Immiscible Layer Elevation: (A)-(B)= A [fl< msl (yes/no)
(D) Depth lo Groundwater. I c, 'if I ft. WELL VOLUME DATA
(E) Groundwater Elevation: (A)-(0)= 7 9 9. O?i msl (yes/no) DIA. or PIP[ (in.) VOLUME IN GAL/rt.
1.0 0.041
(r) Total Well Depth = c2.~~ ft. 2.0 0.163
ID-5 j
3.0 0.367
(G) Length of Water Column: (f)-(0)= ft. 4.0 0.653
I .:J 5.0 1.020
Cosing Volume = (G) x Volume in goi./11.= gols. 6.0 1.470
t.16thod of Well Evacuation 211~p Start Time: I 3 / C, TO CONVERT GAL/FT TO LITERS/FT, MULTIPLY ABOVE FIGURES BY
Method of Sample Collection E1!!1G2 Time:
3.6 LITERS/GALLON. ,
I ";J3'2
Chain-of-Custody form Started (r9no)
FIELD ANALYSES
1st Volume 2nd Volume 3rd Volume 4th Volume 5th Volume
Volume Purged (gallons) /. 7 '<.t/ S-1
Time (mililary) I -~7 1 I 'J. 7q, I~">\
pH {S.U.) ~·.n· '' <, -
Sp. Cond. (umhos/cm) S ~HD , Lill'\ <;-,' 7 (')
Water Temp. ("C) I-, 17 ,,
Odor (subjective)• H ·u· ~
Turbidity (subjective)" . I ' I
• (1 )None (2)Slighl (3)Moderale (4)Slrong
" (1 )Clear (2)Slighlly Turbid (3)Moderalely Turbid (4)Very forbid (5)Exlremely Turbid
Comments/Observations/Recommendations:
FORM COMPLETE:A::: J~ 1%ffei~I I D[
O& F Form48 {3/94)
00002R
~~~~ LABORATORY ANALYSIS REPORT
Explanation of Symbols and Abbreviations
The following defines common symbols and abbreviations used in reporting technical data:
RDL Report Detection Limit MDL Method Detection Limit
TOP Top of Pipe MSL Mean Sea Level
TNTC Too Numerous To Count MPN Most Probable Number
BTU British Thermal Units NTU Nephelometric Turbitity Units
C Degrees Centigrade F Degrees Fahrenheit
umhos/cm micromhos/cm meq milliequivalents
kg
mg
I
ul
lb
ft
mg/I, mg/kg
ug/1, ug/kg
wt%
<
kilogram(s) g gram(s)
milligram(s) ug microgram(s)
liter(s) ml milliliter(s)
microliter(s) m3 cubic meter(sl
pound(s) ft3 cubic foot(feet)
foot(feet) TIC Tentatively Identified Compounds
Units of concentration in milligrams per liter for liquids and milligrams per kilogram for solids.
Also referred to as Parts Per Million or "ppm" when the assumption is made that the specific
gravity or density is one (1 g/ml).
Units of concentration in micrograms per liter for liquids and micrograms per kilograms for
solids. Also referred to as Parts Per Billion or "ppb" when the assumption is made that the
specific gravity or density is one (1 g/ml).
Units of concentration expressed on a weight/weight basis (e.g. grams per 100 grams).
Less Than -The number following the sign is the limit of quantitation, the smallest amount of
analyte that can be reliably determined using this test.
> Greater Than
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Data Qualifiers: I
A
B
C
E
J
p
X
•
TIC is a possible a\dol-condensation product resulting from sample extraction. (Organics)
Analyte also detected in the method blank.
Amenable Cyanide is a negative value due to an unknown interference.
Estimated concentration due to interference.
Estimated value below RDL or estimated value for TIC. (Organics)
Concentration difference between primary and confirmation columns > 25%. (Organics)
The lower result is reported.
Matrix interference which requires dilution or prevents the reporting of a result. Detection limits
have been adjusted where applicable.
Defined in report comments .
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Solid samples (i.e. soil, sludge, and solid waste) are reported on a dry weight basis unless otherwise noted.
Test results relate only to the sample tested. Clients should be aware that a critical step in a chemical or I
biological analysis is the collection of the sample. Unless the sample analyzed is truly representative of the
bulk of the material involved, the test results will be meaningless. If you have any questions regarding the
proper techniques of collecting samples, please contact us. However, we cannot be held responsible for I
sample integrity unless sampling has been performed by a member of our staff.
WARRANTY AND LIMITATION OF LIABILITY -The accuracy of all analytical results is warranted for the 1 sample as it is received by the laboratory. Warranty for the integrity of the sample begins at the time it is
placed in the possession of authorized Davis and Floyd, Inc. Laboratories personnel. All other warranties,
expressed or implied, are disclaimed. Liability is limited to the cost of the analysis.
Davis & Floyd, Jnc. I PO Drawer 428 I Greenwood, SC 29648 I 816' E. Durst Avenue I Greenwood, SC 29649 I [phone] I Fax [phone]
0001)?'7
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I Attachment 3
I Selected Water-Quality Plots
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I Kubal-Furr & Associates
-------------------Inner Tier Combined Influent TOC Data
ITCI TOC Data
4000 ~--------------------------------------,
3000
~ ~ 2500
Cl E ,._.
C: 0 ·.:; 2000
~ ... C: ., u C: 8 1 500 ------- ----- ----
1000 ------------------- -- ----------------
500
0+------t------+-------,.---------,.-------,-------,----
1/1/93 1 /1 /94 1 /1 /95 1 /1 /96
Date
12/31/96 12/31/97 12/31 /98
-------------------
Location l2ate.
ITCI 11 /29/94
3/7/95
5/18/95
8/22/95
11 /29/95
1/16/96
4/15/96
7/12/96
10/31 /96
1 /17 /97
4/29/97
7/22/97
10/28/97
1/22/98
5/7/98
7/21/98
10/20/98
1 /14/99
4/8/99
'ilal.ue.
2330
1800
1000
209
52
1100
1070
550
840
603
1560
1430
1110
99
1310
596
550
665
1510
Unit
mg/L J
mg/L
mg/L JL
mg/L
mg/L Z
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
ITCI Ethylene Glycol Data
~ _,
----C)
ITCI Ethylene Glycol Data
2500 ~------------------,
2000
5 1500
C
0 ·;;
~
'c: 1000 · · ·
Q) u C 0 u
500 · · · · · · · ·
0+----'f-----+-----r------J--
11 /29/94 11 /29/95 l 1 /28/96 11 /28/97 11 /28/98
Date
-------------------Monitor Well V-23 TOC Data
V-23 TOC Data
12000 ~---------------------------------------,
C: .g 6000 ------- -
~ ... C: Q) u C: 0 u 4000
2000 ·-----------
0-1-------+-----f-------+-----~-----+------+-----+--_J
1/1/85 1/1/87 12/31/88 12/31/90 12/30/92 12/30/94 12/29/96 12/29/98
Date
-------------------
Monitor Well V-23 2-Butanone Data (MEK)
Locatio □ Date. 'ialLLe. Unit
V-23 8/3/89 1.1 mg/L V-23 2-Butanone (MEK) 11/9/89 0.45 mg/L
1 /5/90 0.37 mg/L
2/23/90 0.038 mg/L 4
8/8/90 0.56 mg/L
11/7/90 0.01 mg/L u 3.5 ------------------------------------------------
2/5/91 0.66 mg/L
5/3/91 0.46 mg/L 3 -------------------------------· ---------------
~
8/9/91 0.04 mg/L u ..J ' Cl 11/4/91 0.05 mg/L u E 2.5 -----------------------------------------------
~
2/4/92 0.2 mg/L C 0
5/5/92 0.2 mg/L u ·;:; 2 - - - - - - - ----- - - - - ---- - - ------------------------.. ~
8/7/92 0.8 mg/L -C
Q) 1.5 -------------------------------------------11/6/92 0.1 mg/L u u C
2/3/93 0.05 mg/L u 0 u --------------
5/5/93 0.25 mg/L u
8/6/93 0.044 nig/L 0.5 11 /3/93 0.01 mg/L u
2/2/94 0.25 mg/L u 0
8/5/94 0.52 mg/L 6/1 /89 6/1/91 5/31/93 5/31 /95 5/30/97
3/8/95 0.01 mg/L <
8/24/95 0.767 mg/L > Date
1 /16/96 3.6 mg/L
7/12/96 0.5 mg/L
1/17/97 0.591 mg/L
7/22/97 0.01 mg/L <
1/22/98 0.164 mg/L
7/21/98 0.466 mg/L
1/14/99 0.34 mg/L
-------------------
Monitor Well V-23 Acetone Data
Locatioo 12.ate 'La1ue. Unit
V-23 8/3/89 0.1 mg/L u
11 /9/89 0.295 mg/L
1/5/90 0.3 mg/L
2/23/90 0.34 mg/L V-23 Acetone Data 8/8/90 0.31 mg/L
11/7/90 0.01 mg/L u
2/5/91 0.52 mg/L 1.4
5/3/91 0.53 mg/L
8/9/91 0.48 mg/L 1.2 ----------------------------------------------
l l /4/91 0.53 mg/L ~ _, 1 ---------------2/4/92 0.08 mg/L B ----Cl
5/5/92 0.2 mg/L u E
';;; 0.8 ---------------------
8/7/92 1.1 mg/L E 0 '.;:; 11/6/92 0.14 mg/L "' b 0.6 ----------------------- - -- -- - - - -
2/3/93 0.05 mg/L u C: Q)
5/5/93 mg/L B u 1 § 0.4 -------· --------------
8/6/93 0.025 mg/L u
11/3/93 0.01 mg/L u 0.2 ------
2/2/94 0.36 mg/L
8/5/94 0.52 mg/L 0
3/8/95 0.01 mg/I 6/1 /89 6/1 /91 5/31/93 5/31/95 5/30/97
8/24/95 0.648 mg/I J Date 1/16/96 0.487 mg/L
7/11/96 1.1 5 mg/I
l /17 /97 0.818 mg/I
7/22/97 0.05 mg/I <
l /22/98 0.01 mg/I <
7/21/98 1.22 mg/I J
1/14/99 0.005 mg/L <
-------------------
Monitor Well V-23 Benzene Data
Location Date. 'lalue. Unit
V-23 8/3/89 0.05 mg/L u
11/9/89 0.005 mg/L u
1 /5/90 0.019 mg/L J
2/23/90 0.031 mg/L V-23 Benzene Data
8/8/90 0.02 mg/L u
11/7/90 0.013 mg/L 0.25 2/5/91 0.022 mg/L J
5/3/91 0.013 mg/L J
8/9/91 0.04 mg/L u 0.2 ---------------------- - ------------------------------
11/4/91 0.015 mg/L J ~
2/4/92 0.012 mg/L J ...J --.. 0)
5/5/92 0.071 mg/L J 5 0.15 --------------------- - -------------------------
8/7/92 0.05 mg/L u C: 0
11 /6/92 0.017 mg/L J ·.;:;
"' ~
2/3/93 0.006 mg/L J ... 0.1 C: ----------------------------------------------" 5/5/93 0.25 mg/L u u C:
8/6/93 0.004 mg/L J 0 u
11/3/93 0.022 mg/L 0.05
2/2/94 0.25 mg/L u
8/5/94 0.022 mg/L J
3/8/95 0.011 mg/I < 0
8/24/95 0.0293 mg/I 6/1 /89 6/1/91 5/31/93 5/31/95 5/30/97
1 /16/96 0.0193 mg/L Sample Date
7/11/96 0.0291 mg/I
1/17/97 0.0178 mg/I
7/22/97 0.02 mg/I
1/22/98 0.0104 mg/I
7/21/98 0.0207 mg/L
1/14/99 0.014 mg/L
-------------------
Monitor Well CC-33 Benzene Data
Locatio□ Date. 'Lallle Unit
CC-33 8/4/89 0.085 mg/L
11/8/89 0.08 mg/L CC-3 3 Benzene Data 2/14/90 0.081 mg/L
5/4/90 0.079 mg/L 0.14
8/9/90 0.096 mg/L
11 /6/90 0.073 mg/L
2/6/91 0.095 mg/L 0.12
5/2/91 0.089 mg/L
8/8/91 0.08 mg/L
11/4/91 0.14 mg/L 0.1 ------------- - --. ----------------- - -----------------
2/4/92 0.11 mg/L
~ 5/4/92 0.11 mg/L ...J
---8/7/92 0.1 mg/L 0)
.§, 0.08 ----------------
11 /5/92 0.086 mg/L C 0 2/3/93 0.052 mg/L .:;
~ 5/5/93 0.055 mg/L ..,
a3 0.06 -----------------8/5/93 0.059 mg/L u C
11 /2/93 0.055 mg/L 0 u
2/2/94 0.045 mg/L
8/4/94 0.026 mg/L 0.04
3/9/95 0.014 mg/L
8/24/95 0.0176 mg/L
1/17/96 0.01 mg/L 0.02 -----------------------------------------
7/12/96 0.0128 mg/L
1/17/97 0.005 mg/L <
7/22/97 0.01 mg/L 0
1/22/98 0.005 mg/L 6/1/89 6/1/91 5/31/93 5/31 /95 5/30/97
7/21/98 0.005 mg/L < Date
1 /14/99 0.005 mg/L <
-------------------Monitor Well K-28 TOC Data
K-28 TOC Data
8000.00 ---------------------------------------,
7000.00 ---------------------------- -- ------------------------------------------------
6000.00
-~ 5000.00 --------
~ ~
C: .g 4000.00 - ---------
"' ~ +-' C: (I) g
0 u
3000.00 -------- -- ---------- ---------------------- ---- -------------------------------------------
2000.00 -----------
1000.00 ------
0.00 -l--+--+.__---+----+----+------,------+---=-+-.:._.....::::~~ .. 4Mi'~~,._____J
9/1/81 9/1/83 8/31/85 8/31/87 8/30/89 8/30/91 8/29/93 8/29/95 8/28/97
Date
-------------------
Monitor Well K-28 Benzene Data
Locatio□ llate. ~ Unit
K-28 8/4/89 0.022 mg/L
11/9/89 0.005 mg/L u
1/4/90 0.015 mg/L K-28 Benzene Data 2/19/90 0.025 mg/L u
5/4/90 0.018 mg/L
8/8/90 0.03 mg/L 0.03
11/6/90 0.015 mg/L
2/6/91 0.019 mg/L
5/3/91 0.014 mg/L J 0.025 -------------------------------------
8/8/91 0.017 mg/L
11/4/91 0.03 mg/L J ~
2/4/92 0.017 mg/L ....J 0.02 - --------- - - - - - ----- ----- - - - ------- - - - ------ --- --- -' Cl 5/5/92 0.017 mg/L J E ~
8/7/92 0.019 mg/L C
11/6/92 0.009 mg/L J .g 0.015 - - - - - - - ------ -
I!!
2/3/93 0.009 mg/L J ... C .,
5/5/93 0.014 mg/L u C
8/6/93 0.015 mg/L 0 0.01 u
11/3/93 0.011 mg/L
2/2/94 0.014 mg/L
8/8/94 0.018 mg/L 0.005 --- ---- - - - - - ------- - - - - - - - - -- -------- ------------
3/9/95 0.006 mg/L
8/23/95 0.0205 mg/L 0 1/16/96 0.0086 mg/L
7/11/96 0.0149 mg/L 6/1 /89 6/1/91 5/31 /93 5/31/95 5/30/97
1/17/97 0.005 mg/L < Date
7/22/97 0.01 mg/L
1/22/98 0.007 mg/L
7/21/98 0.0126 mg/L
1/14/99 0.01 mg/L
- - - - - - - - - - - - - -·-- - - -
HH-48 TCE Data
Location Qare 'ilalue. l.1ai!.
HH-48 8/3/89 0.16 mg/L
11/7/89 0.14 mg/L
2/5/90 0.005 mg/L u
5/1 /90 0.17 mg/L
8/2/90 0.15 mg/L HH-48 TCE Data
11 /2/90 0.15 mg/L
2/1/91 0.15 mg/L
5/2/91 0.12 mg/L 0.25 ·
8/2/91 0.01 mg/L u
11/1/91 0.16 mg/L
2/3/92 0.16 mg/L 0.2 ----------------
4/30/92 0.15 mg/L
8/3/92 0.18 mg/L
~ 11/3/92 0.22 mg/L E ..J
---2/1/93 0.15 mg/L 0) E 0.15
5/3/93 0.18 mg/L ~
C: 0 8/2/93 0.2 mg/L .:;
"' 11/1/93 0.22 mg/L E ~ ... C:
1/31/94 0.2 mg/L ., 0.1 . . - - - - -
. ---------u C:
8/1/94 0.16 mg/L 0 u
8/1/94 0.01 mg/L
3/8/95 0.17 mg/L 0.05 .. .. ----------------------------------------·
8/23/95 0.222 mg/L
1/17/96 0.165 mg/L
7/12/96 0.179 mg/L
1/17/97 0.15 mg/L O·
7/22/97 0.09 mg/L 6/30/89 6/30/91 6/29/93 6/29/95 6/28/97
1/22/98 0.101 mg/L Date 7/21/98 0.08 mg/L
1 /14/99 0.088 mg/L
-------------------
HH-77 TCE Data
Locatio□ Date. 'ial.ue. Unit HH-77 TCE Data
HH-77 8/3/89 0.008 mg/L
8/2/90 0.04 mg/L 0.4
8/2/91 0.13 mg/L 0.35 ---------------------
8/3/92 0.067 mg/L
8/2/93 0.12 mg/L ~ 0.3 ---------------------..J ...._
8/1/94 0.12 mg/L Cl
.§. 0.25 -------------8/23/95 0.332 mg/L C:
1/17/96 0.187 mg/L 0 0.2 ·;:; ------------
"' 7/12/96 0.383 mg/L ~ ...
C: 0.15 -------------------------1/17/97 0.224 mg/L ., u
7/22/97 0.26 mg/L C: 0 0.1 -----------u
1/22/98 0.0754 mg/L
7/21/98 0.225 mg/L 0.05 ---------------------------------- - -
1/14/99 0.13 mg/L 0
6/1/89 6/1/91 5/31/93 5/31/95 5/30/97
Date