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HomeMy WebLinkAboutNCD003446721_19970201_Celeanse Corporation - Shelby Fiber_FRBCERCLA RA_OU-1 Semiannual Report July - December 1996-OCRI I I I I I I I I I I I I I I I I I I • Operable Unit 1 Semiannual Report July 1996 -December 1996 Hoechst Celanese Corporation Shelby, North Carolina RECEIVED FEB 191997 SUPERFUND SECTION Document Control No. 026SB-0058 Submitted to U.S. Environmental Protection Agency Region IV Atlanta, Georgia Prepared/or Hoechst Celanese Corporation Shelby, North Carolina February 1997 Kubal-Furr & Associates I I I I I I I I I I I I I I I I I I I Contents ~· Introduction .................................................... l Work Performed ................................................ 3 3rd Quarter 1996 ......................................... · ..... 3 4th Quarter 1996 .............................................. 4 System Performance ............................................... 6 Inner and Outer Tier Extraction Rates ................................ 6 Ground-Water Movement ........................................ 7 Treatment Efficiencies ................................ ; ......... 9 Maintenance Activities .......................................... 9 Analytical Test Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 Data-Quality Assessment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 Discussion of Analytical Test Results ................................ 12 Review of Selected Historical Water-Quality Data . . . . . . . . . . . . . . . . . . . . . . . 13 Closing Comments .............................................. 16 Table l. Table 2. Table 3. Table 4. Table 5. Table 6. Table 7. Tables Sampling Matrix-Hoechst Celanese-Shelby, NC Inner Tier Production Data (July '96 -Dec '96) Outer Tier Production Data (July '96 -Dec '96) Inner/Outer Tier TOC Data (July '96 -Dec '96) Semiannual Maintenance Summary (July '% -Dec '96) Summary of Selected Water-Quality Constituents (3rd Quarter 1996) Summary of Selected Water-Quality Constituents (4th Quarter 1996) i I I I I I I I I I I I I I I I I I I I Figures Figure 1. Site Plan Showing Monitoring Locations and Geologic Cross Sections Figure 2. Potentiometric Surface Map-Shallow Saprolite-July 11, 1996 Figure 3. Potentiometric Surface Map-Deep Saprolite/Upper Bedrock-July 11, 1996 Figure 4. Hydrogeologic Cross Section A-A', July 11, 1996 Figure 5. Hydrogeologic Cross Section B-B', July 11, 1996 Figure 6. Potentiometric Surface Map-Shallow Saprolite--October 31, 1996 Figure 7. Potentiometric Surface Map-Deep Saprolite/Upper Bedrock-October 31, 1996 Figure 8. Hydrogeologic Cross Section A-A', October 31, 1996 Figure 9. Hydrogeologic Cross Section B-B', October 31, 1996 Attachments Attachment 1. Operation and Maintenance Data (July '96 -Dec '96) Attachment 2. QA Summary Report and Analytical Data for the July 1996 Sampling Event Attachment 3. QA Summary Report and Analytical Data for the October 1996 Sampling Event Attachment 4. Selected Water-Quality Plots ii I I I I I I I I I I I I I I I I I I I Introduction Hoechst Celanese Corporation (HCC) is currently operating a long term remedial action (LTRA) system at its Shelby, North Carolina facility. This system, designated as Operable Unit I (OU-I) in the Record of Decision (ROD), consists of two ground-water extraction and treatment systems identified as the Inner Tier and Outer Tier systems. OU-1 became operational in August 1989. The OU-1 Inner Tier system was designed to extract contaminated ground water from around a former source area which was remediated as a separate operable unit (OU-2) with its own ROD. The Outer Tier system was designed to provide hydraulic control over ground water near the property boundary to prevent the off-site migration of any constituents from the former OU-2 source area. The location of the Inner and Outer Tier systems, the former OU-2 source area, and the ground-water monitoring points are shown on Figure 1. In the OU-I Annual Operating Status Report dated September 1995, a recommendation was made to modify the monitoring locations, frequency and parameter list based on a detailed evaluation of the water-quality database assembled for the HCC LTRA. This recommendation was reviewed by the EPA and the State of North Carolina, and approval was given to modify the sampling matrix beginning with the 1st Quarter of 1996. Approval was also given at the time to change the reporting frequency from quarterly to semiannually. The current report represents the Third semiannual report prepared under the new reporting schedule and the second since modification of the sampling matrix. Kubal-Furr & Associates (KF&A) has prepared this semiannual OU-1 operating summary report for submittal to the EPA on behalf of HCC. It covers the period from July 1, 1996 through December 31, 1996 and includes information on system performance and the results of analytical testing of samples collected between July 11-12, 1996 and October 31-November 1, 1996. A summary of the significant events occurring during the reporting period include the following: • A meeting was held with the EPA in Atlanta, and a subsequent telephone conference was held with the EPA and the State of North Carolina Superfund Branch to discuss the scope of a partial deletion petition for parts of the Shelby site. This petition was submitted to the EPA and the State on December 4, 1996, and requested removal of the OU-1 Outer Tier Kubal-Furr & Associates/Page 1 OU-I Semiannual Report (July '96-Dec '%) Hoechst Celanese Corporation-Shelby, North Carolina I I I I I I I I I I I I I I I I I I I and the OU-2 former source area from the NPL. HCC is awaiting EPA's response to the petition. • The PEW extraction well system (also known as the F-Well extraction system) was shut down during the reporting period and well PEW-2, which was found to be improperly constructed, was overdrilled and properly abandoned. The F-Well system is a non- CERCLA related issue which was installed to recover Dowtherm following its discovery in monitor well F-55 in August of 1991. The system will be allowed to equilibrate for six months at which time it will be resampled. The EPA and the State have agreed to include PEW-related monitoring results in future OU-1 semiannual reports rather than prepare a separate report of findings just for the F-Well system. • Due to declines in production from the Inner Tier extraction system, the individual wells comprising the system were rehabilitated during December 1996. The work consisted of shocking the wells with an HTH solution, reworking and cleaning the screens, and redeveloping the sand pack. • The SBR (sequencing batch reactor) which treats recovered Inner Tier ground water was shut down during the period from August 29 -September 5, 1996 to replace a broken air diffuser. Kubal-Furr & Associates/Page 2 OU-] Semiannual Report (July '96-Dec '96) Hoechst Celanese Corporatio/'1--Shelby, North Carolina I I I I I I I I I I I I I I I I I I I Work Performed As part of the OU-1 remedy, samples are collected at selected monitor wells and at points in the ground-water treatment system. The frequency of analysis and the parameters to be analyzed are summarized in the sampling matrix (Table 1). A description of the work performed during this reporting period is provided below. No domestic supply wells were sampled during the reporting period. As noted in the previous semiannual report, all off-site domestic supply wells that had been used for ground-water monitoring have been plugged back at the owners request as part of an HCC Voluntary Initiative to provide the surrounding residents with county water. 3rd Quarter 1996 During July 1996, water levels were measured in a total of93 monitor wells, extraction wells, and piezometers. Water-quality samples were collected from 13 monitor wells and 4 process points to be analyzed for the parameters summarized in Table 1. The samples were collected and analyzed by Shealy Environmental Services of Columbia, South Carolina. Monitor Well Samplinv Thirteen monitor wells were analyzed in the field for pH, temperature and conductance; and, by the laboratory for volatile organics using EPA Method 8260A. Additionally, samples from monitor wells K-28 and V-23 were analyzed by the laboratory for TOC using EPA Method 415.1. Process Point Samplinv Samples of Inner Tier (IT) influent and effluent, and Outer Tier (On influent and effluent were collected for analysis of volatile organics by Method 8260A. The Inner Tier influent and effluent samples were also analyzed by the laboratory for TOC by Method 415.1, and for ethylene glycol byGC/FID. During the reporting period, influent and effluent samples from the Inner Tier and the Outer Tier were also collected by HCC personnel for analysis of TOC by the HCC on-site laboratory. Kubal-Furr & Associates/Page 3 OU-1 Semiannual Report (July '96-Dec '%) Hoechst Celanese Corporatioll-She/by, North Carolina I I I I I I I I I I I I I I I I I I I These samples are collected weekly to evaluate treatment efficiency, and the results are contained in the O&M repons provided in Attachment I. These results are also summarired in Table 4. 4th Quarter 1996 During October 1996, water levels were measured in a total of 92 monitor wells, extraction wells, and piezometers. Water-quality samples were collected from 2 monitor wells, and 2 process points and analyzed for the parameters summarized in Table 1. The samples were collected by Shealy Environmental Services who also performed the analyses. Monitor Well Sampling Monitor wells K-28 and V-23 were sampled during the 2nd Quarter sampling event. These wells were analyzed in the field for pH, temperature and conductivity; and, by the laboratory for TOC by Method 415.1. Process Point Sampling Samples of Inner Tier influent and effluent were collected for analysis of TOC by Method 415.1 and volatile organics by EPA Method 8260A. The Inner Tier influent and effluent samples were also analyzed for ethylene glycol by GC/FID. Kubal-Furr & Associates/Page 4 OU-1 Semiannual Report (July '96-Dec '96) Hoechst Celanese Corporation-Shelby, North Carolina I I I I I I I I I I I I I I I I I I I System Performance Detailed records of system maintenance are kept by HCC and are summarized monthly. The monthly records for the current reporting period are contained in Attachment 1. Summaries of physical operating data for the Inner and Outer Tier extraction well systems are presented in Tables 3 and 4, respectively. Inner and Outer Tier Extraction Rates During the reporting period, the Inner Tier wells extracted a total of 351,411 gallons. Inner Tier flows ranged from a low of 47,773 gallons in September, to a high of 77,254 gallons in July. Pumping from the Inner Tier wells is limited by the capacity of the SBR treatment system, which is designed to process about 2500 gallons of water per day. With 184 days in the reporting period, the optimum pumping from the Inner Tier would have been some 460,000 gallons. Based on the pumpage during the reporting period, the Inner Tier extraction system was producing at a rate of about 76% of the optimum rate. Part of the poor performance can be explained by ihe downtime during replacement of the SBR air diffuser. Also, there has been a gradual decline in production from the Inner Tier which required rehabilitation of all wells during December 1996. The Outer Tier wells extracted 13,242,724 gallons during the reporting period. The flow from the Outer Tier system ranged from a low of 2,083,059 gallons in October to a high of 2,301,452 gallons in August. It is important for the Inner Tier system to extract and treat contaminated ground-water at a rate as near the design capacity as possible due to the lengthy clean-up times involved with the remedy. The Outer Tier system, however, needs to be evaluated somewhat differently than the Inner Tier. The Outer Tier is extracting water primarily to maintain hydraulic control near the property boundary in order to prevent off-site migration of former OU-2 source area constituents. Therefore, the primary evaluation criteria for the Outer Tier system needs to be drawdown along the perimeter of the site. The actual pumping rates and treatment efficiencies, while providing useful data, are of lesser importance than the demonstration of hydraulic control. A description of the techniques used to evaluate the ability of the Outer Tier to control ground-water movement along the perimeter is described below. Kubal-Furr & Associates/Page 5 OU-I Semiannual Report (July '96-Dec '96) Hoechst Celanese Corporation--Shelby, North Carolina I I I I I I I I I I I I I I I I I I I Ground-Water Movement The purpose of the OU-1 remedial design was to extract contaminated ground water from the fonner OU-2 source area and to provide hydraulic control at the property boundary to prevent the off-site migration of constituents. Along with the water-quality data, one of the best ways to evaluate system perfonnance in terms of the above objectives is to construct potentiometric surface maps which allow inferences as to the direction of ground-water movement. In order to accurately predict the direction of ground-water movement, water-level measurements were collected from all accessible monitor wells, extraction wells and piezometers during each of the 3rd and 4th Quaner sampling events. These data were used to construct the potentiometric surface maps and hydrogeologic cross sections from the July 11, 1996 water levels (Figures 2, 3, 4, and 5) and from the October 31, 1996 water levels (Figures 6, 7, 8,and 9). The shallow saprolite maps (Figures 2 and 6) show the water-level contours and direction of ground-water movement in the uppermost water-bearing zone beneath the site. The direction of movement in this zone is to the east from upgradient areas along NC 198, towards discharge areas along the intermittent, unnamed tributaries of Buffalo Creek. Drawdown and a capture zone are apparent on these figures situated around the Inner Tier extraction system, and along the Outer Tier system. An attempt was made to separate the uppermost water-bearing zone from the deeper saprolite and upper bedrock zone. While these maps (Figures 3 and 7) present a reasonable picture of ground-water movement in this zone, it should be pointed out that these maps are giving a somewhat more generalized picture of ground-water movement because of the well construction techniques used in many of the wells and piezometers. The typical construction of these wells was to have relatively long screens (20-40 ft) and extremely long sand packs in the annular space above the screens (up to 60-ft). As a result, the lower saprolite/upper bedrock maps have a number of composite head values measured along a longer screened area. However, the maps are useful for determining the general direction of ground-water movement. The lower saprolite/upper bedrock maps show movement toward the east from the upgradient areas west of the plant. These maps also show the drawdowns and capture zones along the Outer Tier extraction well system along the east property boundary. These maps indicate that the Outer Tier system was exening hydraulic control along the property boundary during the 3rd and 4th Kubal-F"" & Associates/Page 6 OU-1 Semiannual Report (July '96--Dec '96) H~chst Celanes~ Corporation-Shelby, North Carolina I I I I I I I I I I I I I I I I I I I Quarters of 1996. Less control was noted along the northern portion of the Outer Tier, and well OT-8 has been experiencing problems with siltation which HCC has been unable to correct even following redevelopment of this well. It appears that OT-8 is experiencing problems similar to those which caused the replacement of OT-I and OT-2. To confinn inferences made about the direction of movement and hydraulic control exerted by the Inner and Outer Tier systems, two hydrogeologic cross sections each were constructed for the July and October data sets (Figures 4 and 5, and 8 and 9, respectively). The locations of the cross sections are shown on the site base map, Figure 1. There is one east-west cross sections (A-A') constructed through the plant from upgradient areas west of the plant to downgradient, off-site areas east of the plant. The other cross section (B-B ') is oriented north-south, and is situated along the Outer Tier extraction well system. The hydrogeologic cross sections are very similar for the two measurement periods and show a general direction of movement in the saprolite and upper bedrock from upgradient areas west of the plant toward downgradient areas to the east. No appreciable downward hydraulic gradients are apparent on these maps except in the vicinity of the extraction wells, and the movement in the saprolite and shallow bedrock is predominantly horizontal across the site. The Inner Tier capture zone is shown on Figures 4 and 9. These figures show that the Inner Tier is extracting water from beneath the former OU-2 source area in accordance with the remedial design. The Outer Tier capture zone is shown on all of the cross sections and it can be inferred to extend entirely beneath the plant in cross sections A-A'. Cross section B-B' indicates that the Outer Tier wells are exerting hydraulic control along the eastern property boundary from near DD-58 in the south to near PZ-12 at the northern boundary. Kubal-Fu" & Associates/Page 7 OU-I Semiannual Report (July '96--Dec '96) Hoechst Celanese Corporation-Shel/Jy, North Carolina I I I I I I I I I I I I I I I I I I I Treatment Efficiencies Two aspects of the extraction system performance were reviewed for this annual report: the production rates achieved during the year, and the removal efficiencies for TOC from the Inner Tier and from the Outer Tier systems. Presented in Table 5 is a summary of the treatment system effectiveness of the Inner Tier and of the Outer Tier in removing TOC during the reporting period. These summaries were prepared from the water-quality data collected weekly by the HCC on-site laboratory as presented in the monthly operating summaries (Attachment 1). During the reporting period, the Inner Tier average removal efficiency for TOC was 94%, with an average influent concentration of 1664 ppm (parts per million), and an average effluent concentration of 98 ppm. Removal rates for TOC from the Outer Tier treatment system were calculated to be 53%, lower than the Inner Tier but in keeping with historical values. The average influent concentration during the reporting period was 9 ppm, and the average effluent concentration was 4 ppm. The percent reduction of TOC through the Outer Tier treatment system is not as high as that for the Inner Tier because of the much lower Outer Tier influent TOC. The Outer Tier appears to be reducing TOC as well as can be expected. Maintenance Activities Low flow from the Inner Tier wells is a chronic problem requiring frequent maintenance. The actions taken to rectify the low flow problems consisted of replacing bladders, timers, air lines and such, adjusting the controls and flow rates, and cleaning the strainers. The individual IT wells were also rehabilitated during December 1996 as described in the Introduction. Specific actions taken at individual wells during the reporting period are contained in the monthly operating summaries (Attachment 1 ). A summary of Inner Tier maintenance incidents is summarized in Table 5. Replacing bladders at the IT weUs was the most frequent maintenance activity during the reporting period, with IT-2 and IT-5 requiring 3 bladder replacements each. IT-SR experienced the most frequent number of maintenance activities, principally related to problems with the Hammerhead pump. This pump problem has been noted in earlier operational reports as well. Kubal-Furr & Associates/Page 8 OU-1 Semiannual Report (July '96-Dec '96) Hoechst Celanese Corporation-Shelby, North Carolina I I I I I I I I I I I I I I I I I I I No unusual operational problems were experienced during the reporting period in the Outer Tier recovery well system. Well OT-6A experienced the most numerous maintenance requests followed by OT-5. Adjusting the flow was the most frequent maintenance request during the reporting period, principally at wells OT-IR and OT-2R. Kubal-Furr & Associates/Page 9 OU-1 Semiannual Report (July '96-Dec '96) Hoechst Celanese Corporation-Shelby, North Carolina I I I I I I I I I I I I I I I I I I I Analytical Test Results The analytical test results for the 3rd and 4th Quarter sampling events were evaluated using method specific quality control criteria and, for additional guidance when necessary, the EPA's National Functional Guidelines for organic and inorganic data review. The data assessment summary report for the 3rd Quarter sample set is presented in Attachment 2 along with the analytical test results, field sampling logs, water-level measurements, and chain-of-custody forms. Similar information for the 4th Quarter data set is contained in Attachment 3. A summary of selected analytical data for the 3rd and 4th Quarters is presented in Tables 6 and 7, respectively. Data Quality Assessment Regarding sample collection, the sampling logs and field information provided was complete. The chains of custody were incomplete with respect to site specific information concerning client information, etc. Also, several pages of the field notes/logbook were missing signatures and dates and needed to be reissued. These deficiencies did not compromise_ the data quality but they will be corrected in future sampling events. All TOC data and ethylene glycol test results for the 3rd and 4th Quarters met all method acceptance criteria and are considered useable for quantitative purposes. During the 4th Quarter, methylene chloride was reported as present in the field blank. However, the samples associated with this field blank did not require data flags based on their reported concentrations. Therefore, all VOC data met the method acceptance criteria and is considered useable for quantitative purposes. Kubal-Furr & Associates/Page JO OU-I Semiannual Report (July '96-Dec '96) Hoechst Celanese Corporation-Shelby, North Carolina I I I I I I I I I I I I I I I I I I I Discussion of Analytical Test Results Monitor Wells Of the 13 monitor well samples analyzed during the reporting period, only 5 had any volatile organics reported above the detection level. Of these five, only one (V-23) had more than one inilividual constituent reported as present above the detection level. Monitor well V-23, located downgrailient of the former OU-2 source area and just upgradient of the Inner Tier extraction system, reportedly contained acetone (1150 µg/L), benzene (29.1 µg/L), 2-butanone (MEK) (504 µg/L), carbon disulfide (59.1 µg/L) and 2-hexanone (343 µg/L). CC-33 and K-28, adjacent to and just downgradient of the former OU-2 source area, reportedly contained benzene at 12.8 µg/L and 14.9 µg/L, respectively. Mot;1itor wells HH-48 and HH-77, off-site and adjacent to the Elliott residence, reportedly contained trichlorothene (TCE) at concentrations of 179 µg/L and 383 µg/L, respectively. The presence of TCE at this location is thought to be the result of a localized source, unrelated to activities at HCC or the former OU-2 source area. Monitor wells K-28 and V-23 were also analyzed for TOC during the 3rd and 4th Quarters. The V-23 test results were similar for the 3rd and 4th Quarters at 10,400 and 10,800 mg/L, respectively. The TOC test results for K-28 were noted to increase from 17 mg/L to 86 mg/L between the 3rd and 4th Quarters. Process Point Samples 3rd Inner Tier influent and effluent samples were analyzed during the 1st and 4th Quarters for ethylene glycol, TOC, and volatile organics. All volatiles in the Inner Tier effluent sample were below the detection levels. The 3rd Quarter Inner Tier influent sample reportedly contained the volatiles acetone (621 µg/L), benzene (51.2 µg/L), MEK (97.9 µg/L), and chlorobenzene (40.1 µg/L). The 4th Quarter Inner Tier influent sample reportedly contained the volatiles acetone (137 µg/L), benzene (39.9 µg/L), MEK (132 µg/L), carbon disulfide (19.4 µg/L), chlorobenzene (12.7 µg/L), and 2-hexanone (30.9 µg/L). TOC test results for the Inner Tier influent samples were noted to decrease between the 3rd and 4th Quarters from 2600 mg/L to 1560 mg/L, respectively. Inner Tier effluent TOC was reported at 130 mg/Land 116 mg/L for the 3rd and 4th Quarters, respectively. Kubal-Furr & Associates/Page 11 OU-] Semiannual Report (July '96-Dec '96) Hoechst Celanese CorporaJion-Shelby, North Carolina I I I I I I I I I I I I I I I I I I I Review of Selected Historical Water Quality Data Attachment 4 contains plots of selected water-quality constituents for various monitor wells and process points. The choice of locations and constituents was based on a review of the water-quality database, in particular those locations having any meaningful data to plot. In general, only those monitoring locations within a few hundred feet of the former OU-2 source area have any significant number of water-quality constituents reported above the detection limits. In an attempt to assess long-term improvement in water-quality conditions resulting from source removal and ground-water recovery, the following locations and constituents were selected: • Inner Tier Combined Influent TOC and ethylene glycol test results. The Inner Tier TOC continues to fluctuate in a fairly narrow range of from 1500 to 2500 mg/L, and no long- term trends have been established. However, with the exception of the 3rd Quarter test result, the TOC results have been trending downward during the past year and may be an early indication pf some gradual improvement in water-quality conditions. Similarly, the Inner Tier ethylene glycol data have established an apparent downward trend although the database is much smaller than the TOC database and contains several qualified data points. • Monitor Well V-23 TOC, 2-butanone (MEK), and acetone. An attempt to plot benzene did not provide any useful information because more than half the benzene data for V-23 are either below the detection levels or qualified as estimated. The V-23 TOC data began trending downward from a high of 8000 mg/Lin mid-1989 to less than 1000 mg/Lin early 1992. Since that time, the TOC data has shown several wide swings in concentration, and at the present time, no trend has established itself during the past several years. The concentrations for TOC at V-23 were the highest ever reported during the 3rd and 4th Quarters. The V-23 MEK data have generally fluctuated in a narrow range less than 1 mg/L, with 10 of 24 data points below the detection level. The 1st Quarter data showed a spike for MEK at 3.6 mg/L which was questioned in the previous semiannual report. The current value for MEK of 0.504 mg/L is back within expected ranges based on historical trends at this location. Kubal-Furr & Associates/Page 12 OU-1 Semiannual Report (July '96--Dec '96) Hoechst Celanese Corporatum--Shelby, North Carolina I I I I I I I I I I I I I I I I I I I The V-23 acetone test results have generally fluctuated in a narrow range below 0.6 mg/L since 1989. No apparent trend has been established from the reported acetone test results at this monitoring location. • Monitor well CC-33 benzene and chlorobenzene data. The water-quality plots for monitor well CC-33, just south of the Inner Tier capture zone, have shown a continual improvement in water-quality conditions as indicated by these two constituents. In the case of chlorobenzene, this improvement began in late 1989, just after start up of the Inner Tier extraction system. Both benzene and chlorobenzene peaked at about the mid-point in the OU-2 remediation (late 1991), and have continued to decline since that time. • Monitor well K-28 TOC, MEK, acetone and benzene data. TOC, MEK and acetone have all shown a decrease in concentration beginning about the time the OU-2 source remediation began in January of 1991. While benzene has also shown a decline during this period, this trend is not as readily apparent, and for the past three years benzene has been fluctuating in a range of from 0.01 to 0.02 mg/L. • Monitor well HH-48 and HH-77 TCE data. The HH-48 TCE test results have generally fluctuated in a narrow range of from 0.15 to 0.25 mg/L during the past six years, and no apparent trend is evident in the water quality plots. HH-77 had been fluctuating in the range of 0.05 to 0.15 mg/L until the August 1995 sampling event when it peaked at 0.332 mg/L. The subsequent sample for HH-77 (1st Quarter 1996) was below 0.2 mg/L, while the most recent sample (3rd Quarter 1996) is the highest reported value at this location (0.383 mg/L). As noted in an earlier section, the TCE contamination in this area appears to be due to a localized source and not related to past activities at HCC. Kubal-Furr & Associates/Page 13 OU-1 Semiannual Report (July '96-Dec '96) Hoechst Celanese Corporation-Shelby, North Carolina I I I I I I I I I I I I I I I I I I I Closing Comments The extraction well production data and the analytical test results for the monitor wells and process points were generally found to be consistent with historical information, and no unusual or unsuspected contamination was identified during the reporting period. Treatment efficiencies at the Inner Tier for removal of TOC remained consistently greater than 90%, and no volatiles were detected in either the 3rd or 4th Quarter Inner Tier effluent samples. The present report represents the third semiannual report prepared under a revised sampling, analysis and reporting schedule approved by the EPA during its review of the OU-I Annual Report (August 1995). The next sampling events are scheduled for the 1st and 2nd Quarters of 1997, with the next scheduled semiannual report to be submitted to the agency by September 1, 1997. Kubal-Furr & Associates/Page 14 OU-I Semiannual Report (July '96--Dec '96) Hoechst Celanese Corporation-Shelby, Nor1h Carolina - - -- - ----· -- ------- - Table 1. Sampling Matrix-Hoechst Celanese-Shelby 1st Quarter 2nd Quarter 3rd Quarter 4th Quarter Monitoring TOC voe Eth. Glycol TOC voe Eth. Glycol TOC voe Eth. Glycol TOC voe Eth. Glycol Location (415.1) (8260) (GCIFID) (415.1) (8260) (GCIFID) (415.1) (8260) (GC/FID) (415.1) (8260) (GCIFID) Process Points ITCI .J .J .J .J .J .J .J .J .J .J .J .J fTEF .J .J .J .J .J .J .J .J .J .J .J .J OTCI .J .J OTEF .J .J SBAS~dge (Full TCLP) FP Sludge (Full TCLP) Monitor Wells C-49 .J .J K-28 . .J .J .J .J .J .J P-58 .J .J T-35 .J .J V-23 .J .J .J .J .J .J AA-54 .J .J CC-33 .J .J EE-58 .J .J FF-34 .J .J FF-62 .J .J GG-61 .J .J HH-48 .J .J HH-77 .J .J Domestic Suee!l, Wells Lambert11 .J Runyans2' .J .J Notes: 1 / Lambert Well abandoned on February 19, 1996. 2/ Runyans well abandoned on April 16, 1996 Hoechst Celanese-Shelby, NC OU-1 Semiannual Report (July '96 -December '96) - Well IT-1 IT-2 IT-3 IT-4 IT-5 IT-8 IT-7 IT•BR IT-9 • ADF: - -- - - -- - - Table 2. Inner Tier ProducUon Data July '96 •• Dec '96 Hoechst Celanese CorporaUon-Shelby, NC July 1996 August 1996 September 1996 October 1996 Total Total Total Total Gallons AOF' Gallons AOF' Gallons ADF" Gallons ADF" 4,127 133 3,210 104 2,785 93 3,195 103 1,663 54 1,153 37 1,017 34 1,263 4 1 2 392 11 1 868 60 1 582 53 1 558 50 2,205 71 1,860 60 1,189 40 1,374 44 10,735 346 7,073 228 7,126 238 9,496 306 2,745 89 3 125 1 01 2,436 81 3 473 112 4,981 161 4,31-4 139 3,485 116 4,260 137 28,068 905 13,835 446 15,352 512 4,777 154 20,338 656 16,233 524 12,801 427 20 682 667 77,254 52,671 47,773 50,078 Average Daily Flow based on HCC production records (Attachment 1 ). Calculated as IOtal flow divided by Iha number of days in Iha month. ------ - November 1996 Total Gallons ADF" 3,195 107 496 17 822 27 2,138 71 8,783 293 2,860 95 3,681 123 30,470 1,016 12,332 411 64,777 December 1996 July-Dec '96 Total Gallons ~ Total Gallons 3,838 124 20,350 595 1 9 6,187 2 464 79 10 686 2,844 92 11,610 8,246 266 51,459 3 459 112 18 098 4,337 140 25,058 21,905 707 114,407 11 170 360 93 556 58,858 351,411 1/oechst Celanese-Shelby.NC OU-1 Semiannual Report (July '96 -December '96) - - Well OT•1R OT-2(A) OT-3 OT-4 OT-5 OT-6 OT-6A OT-7 OT-8 'AOF: - - -- - - -- - - Table 3. Outer Tier Production Data July '96 -Dec '96 ---- - - - Hoechst Celanese Corporation-Shelby, NC July 1996 August 1996 September 1996 Total Total Total Gallons ADF" Gallons ADF" Gallons ADF" 704,600 22,729 669,658 21,602 846,400 21,547 287,900 9,287 328,800 10,606 308,100 10,270 67 1829 21188 631271 21041 581441 11948 41,937 1,353 40,745 1,314 37,753 1,258 51,594 1,664 53,770 1,735 85,418 2,847 2301226 71427 217 1324 71010 1981833 61628 280,948 9,063 269,362 8,689 244,360 8,145 80,576 2,599 80,522 2,597 76,515 2,551 555 100 17,906 578,000 18,645 527 600 17,587 2,300,710 2,301,452 2,183,420 Average Daily Flow based on HCC production records (Attachment 1}, Calculated es total flow divided by the number of days in the month. October 1998 Total Gallons ADF' 634,400 20,465 286,700 9,248 581186 11877 38,193 1,232 89,838 2,898 1941287 61267 131,807 4,252 76,248 2,460 573,400 18,497 2,083,059 November 1996 December 1996 July-Dae '96 Total Gallons 630,300 303,000 591084 41,335 69,145 1741844 219,529 72,033 565,800 2,135,070 Total Total ADF" Gallons AOF" Gallons 21,010 653,400 21,077 3,938,758 10,100 315,700 10,184 1,830,200 11969 621614 2,020 3691425 1,378 43,692 1,409 243,655 2,305 52,880 1,706 402,645 51828 1821090 5,874 111971604 7,318 233,337 7,527 1,379,343 2,401 72,300 2,332 458,194 18,860 623 000 20,097 3,422,900 2,239,013 13,242,724 Hoechst Celanese-Shelby, NC OU-1 Semiannual Report (July '96 -December '96) - I I I I I I I I I I I I I I I I I I I Date 7 / 1/96 7 /9/96 7/16/96 7 /23/96 7 /29/96 8/6/96 8/12/96 8/20/96 8/27/96 9/24/96 10/1/96 1 0/8/96 1 )/15/96 10/22/96 1 )/29/96 11 /5/96 11/12/96 11/19/96 11/26/96 1 2/3/96 12/9/96 12/17/96 1:!/24/9 6 Average: Table 4. Inner/Outer Tier TOC Data July '96 --December '96 Hoechst Celanese Corporation-Shelby, North Carolina (all results reported in mg/L) Inner Tier Outer Tier Influent Effluent % Reduction Influent Effluent 1323 18 1566 142 91 4 3 2110 35 98 6 7 1580 312 80 3 2 1885 401 79 8 6 1746 124 93 5 3 1714 36 98 5 ; 3 1627 52 97 3 .2 1752 107 94 3 3 2302 80 97 9 6 1312 103 92 9 8 1490 37 98 3 3 1586 49 97 18 6 1719 227 87 39 7 1630 56 97 15 6 1540 37 98 7 3 1440 1 8 99 3 4 2155 59 97 3 8 1581 64 96 6 4 1170 56 95 4 6 1248 70 94 9 3 1874 1 9 99 7 3 1584 69 96 4 3 1664 98 94 9 4 % Reduction 25 33 25 40 40 33 0 33 1 1 0 67 82 60 57 67 57 25 53 Note 1: Inner Tier and Outer Tier Average Influent and Effluent data does not include 07/01 results. Note 2: Inner Tier Average Percent Reduction data does not include 07/01 results. Note 3: Outer-Tier Average Percent Reduction data does not include 07/01, 07/16, 11/12, 11/19 and 12/3 results. Note 4: The S.B.R. was down for maintenance from 08/29/96 to 9/24/96 to replace the diffusers. Hoechst Celanese-Shelby, NC OU-I Semiannunl Report (July '96 -December '96) ------------------- Location ID IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8R IT-9 Total Incidents: OT-1R OT-2R OT-3 OT-4 OT-5 OT-6 OT-6A OT-7 OT-8 Total Incidents: Table 5. Semiannual Maintenance Summary-3rd/4th Quarter 1996 (Number of Incidents Reported) Adj Flow/ Strainer Pump Flow Meter Bladder 1 2 3 1 3 1 1 3 2 1 0 5 3 1 0 NIA NIA NIA NIA 1 1 NIA 1 NIA 3 NIA 1 NIA NIA 0 1 6 0 Total Other Incidents 2 5 2 5 1 1 2 2 2 6 2 3 1 5 8 3 6 19 37 0 1 1 0 0 2 1 3 1 0 1 8 lloechst Celanese-Shelby, NC OU-1 Semiannual Report (July '96 -December '96) ------------------- Table 6. Summary of Selected Water Quality Constituents (3rd Quarter 1996) C-33 K-28 V-23 Total Organic Carbon (mg/L) NA 17 10400 Ethylene glycol (mg/L) NA NA NA Vala tile Organics lua!L/ Acetone ND ND 1150 Benzene 12.8 14.9 29.1 2-butanone (MEK) ND ND 504 Carbon disulfide ND ND 59.1 Chlorobenzene ND ND ND 2-hexanone ND ND 343 Trichloroethane ND ND ND Notes: ND = Constituent not detected/reported as below the detection level NA = Sample not analyzed for indicated constituent(s) HH-48 NA NA ND ND ND ND ND ND 179 HH-77 ITCI ITEF NA 2600 130 NA 550 ND ND 621 ND ND 51.2 ND ND' 97.9 ND ND ND ND ND 40.1 ND ND 133 ND 383 ND ND lloechst Celanese-Shelby. NC OU-rSemiannual Report (July '96 -Dec '96) ·-- - - - - - - - - - - - - - - - - - Table 7. Summary of Selected Water Quality Constituents (4th Quarter 1996) K-28 V-23 ITCI Total Organic Carbon (mg/L) 86 10800 1560 Ethylene glycol (mg/L) NA NA 840 Volatile Organics fug!L/ NA NA Acetone 137 Benzene 39.9 2-butanone (MEK) 132 Carbon disulfide 19.4 Chlorobenzene 12.7 2-hexanone 30.9 Trichloroethane ND Notes: ND = Constituent not detected/reported as below the detection level NA = Sample not analyzed for indicated constituent(s) ITEF 116 ND ND ND ND ND ND ND ND 1/oechst Celanese-Shelby, NC OU-1 Semiannual Report (July '96 -Dec '96) • \ y-49 ~ i \ D \ \ 0 I] • Monitor well Legend -+- 0 Monitor well cluster + Inner Tler Extraction Well ♦ Outer Tler Extraction Well c Domestic Supply Well " Abandoned Inner Tler Well A --I ♦ • A-39 ~ m__ I< PEW Extraction Well Plezometer Stream/Creek HCC Bulldlng/Slructure Abandoned Outer Tler Well PEW-1 t, H-58 H-79 _, Kubal-Furr & Associates -Environmental Consultants- ,/ / I 0 Scale In Feet 400 Figure 1. Sampling Locations Hoechst Celanese Corporation Shelby, North Carolina 800 Monitor well • water Level (ft msQ 0 Monitor Well Cluster .&. Plezometer Legend Inner Tier Extraction Well + (See Table for Water Levels) Outer Tier Extraction Well ♦ (See Table for Water Levels) + PEW Extraction Well ------- --I Stream/Creek ml HCC Building/Structure / Water-Level Contour 7;0 (Dashed where Inferred) ♦ C Abandoned Outer Tier Well Abandoned Inner Tier Well Domestic Supply Well PEW-1 t, H-59 803.40 790 ,,:<' ~ :~;.;~;:, Kubal-Furr & Associates -Environmental Consultants- , I ·I ;, 0 ' ' Inner lier W arer Levels IT-I ; 783.30 IT-2 ; 788.46 IT-3 ; 78146 IT-4 ; 784. 73 IT-5 ; 778.87 IT-6 ; 782.38 IT-7 ; 786.27 IT-8R ; 780.82 IT-9 ; 783.76 Ouca Tier Waca ~vels OT-IR ; 744.34 OT-2R ; 722.55 OT-3 ; 727.51 OT-4 ; 737.49 OT-5 ; 744.78 OT--6 ; 727.45 OT--6A ; 726.83 OT-7 ; 730.49 OT-7A; 772.53 OT-8 ; 754.87 OT-10 77822 , PEW Ware, ~vels PEW-I ; 756.95 PEW-2 ; 79022 PEW-3 ; 802.86 PEW -4 802.67 Scale In Feet 400 800 Figure 2. Potentiomenic Surface Map Shallow Saprolite -July 11, 1996 Hoechst Celanese Corporation Shelby, North Carolina 0 Monitor well cluster + Inner Tier Extraction Well I ♦ Outer Tier Extractlon Well c Domestic Supply Well ,. Abandoned Inner Tier Well 11!11 ♦ 820 HCC Bulldlng/Structure Abandoned Outer Tier Well A-A' Location of geologic cross-sections Kubal-Furr & Associates -Environmental Consultants- 800 _, I 0 Figure 3. Potentiomenic Surface Map Scale In Feet 400 Deep Saprolite and Upper Bedrock-July 11, 1996 Hoechst Celanese Corpo'ration Shelby, North Carolina ' ) 800 850.00 c 830.00 r I I I 810.00 l 790.00 [ I r i 770.00 I ! I i i i 750.00 ~ ,_11_ 730.00 i ' i ! ' I I 71 o.oo I_ A D-27 (828.40) D-35 (828.11) D-56 (82821) Plant Area 820 810 G-50 (809.49) .. • • • J-28 (804.13) • • • W asrewater Treannem Area 800 790 v•A· ' -. t\\j {:\:\{:}\f \{:\:}\:\:: ::::: .. ·. •. ...,,...,..; . 7 . . i-9j;!3_9_ :=:: :: : : : :::::: :=: :: : : : : : : : : : : :.!:::: :=:: :: : : :---. • . -:-: :1) :-:= -:-_ ---=-, :: .-:= :r:=::::: =:-:-- = = = = ===== == = = = = = = = = = = = = = = == == = = :t:: = = == ==== == = == = = = = = = ·-.. --= = = == = = =1= =r = ==-~=~ -:,=-= ~ == = ='= = == == = == = = == = f:---= __ _ _ _________ -------j ---. -------_.. -.• _ _ _ _ ~-__ (778.87 --r--____ f __ _ :-:-:-:-:-:-:----:-:-:-:-:-:-:-:-:-:-:-:-:-:-:-:-:-:-:-:-:-:------:-:-:--1-: : f :-:,-:-:-----;,:---:-:-: f :-:-:-:-:-:-:-:-:-:-,: :: -:-:-:-:-:::: :: : ::::::::::: :i: :: : : : : : : :::::::: :: : := := :: : : : : :::: :-:--7 ----: ::::J-59;~: :{-:-:-:s:0.-: :;:~ : : : : :-::: : : :: : : :=: '.f" :-:-:-:=:-: - , :-_D-88 '.-:-:-_ -:-:-:-:-:-: ,_-:-:-:-'.-'.-_ -:-:-:-:-:-:-:-:-:-:-:-:-:---_ -G-88 9 ___.-...-: :-:-'.-/802.76) '. ___ -:-:-:-:-:-:---r '. · '.-'. -:-:-5:-'.-:•: •:-:-: : ;:: :-: •: • "'I.;. --• -(82816) --------,.----• ----------· ------s26 68) • • -------~ -• ---• -•-t-· ,_·r "· · · · -· · f ---· -l-------"'l. • • :-: •• : : : : : :·:❖ ❖= =l -· · -·-·-· · · · : :· · : : ·:· c·: . :-: :.: : :-:-: : : :·= :=--·-·-··: : : : r-: ·: ·:·:· · : = ·:=s ·· jfu;-:::·=r:·::: = '· .--· ----. -. · -· --------: ·: ·: -: -f •:-: -: · :-· -: · :-: ·: -----: -----· -· · · · · ------J. -· -. ----· -· · -----· --· · · · · ----• -: -: -: -:-: --· -----·· .-----. \ · --· -·. ------· -·(793 181 ·-----•• --~ ------• -·.(760.53) __ - LAND SURFACE i:f :f .r:::un:+ J· ::-:r:: mf .:Hm::::::_,: !:f • ··1.:mt:{; ::·=: ·.r:r-.::n:::\.Jt _.:.··.\:·=·.=:l=:. ]:=;=:rt:. : = •~,¾, ':-:-:-:-:·=---.·-·-·.-.--·.·---j·-·---.·--.· ·----. --... ·---:-:--:-:-1-:-~·-:-:-.--•:•:··--·.-.·-----·----.--------·--.:-:-:-:-:-:-:-:-:i--:•-·--:····-·----.-1--··•:-:-. ~--➔--=-:r----·-·(727.45 ~ . g: .·.-. :: : __ ·. : : .. :.: :: :_: :_: _:l:_: _:: :_ ::: :=: _::: :: _::::::: · :· ·: ! ~=:: :.:.=.-.. :: ~ :.~2~ ::~ _· · == -:\=. : .. ·. :_:_:::_ :_ ~::·:·.-: J :_:_.::t_:_ :?,t;4~"--~~:::r .. :.::.:.:. : r... .. ::=:=:=:=-=-~-~:q~~AA~~~~9::tffl~~-----.·-·-·-·~l:'-~~---.--·-·.-~-----~~~1§l~~---. -. .·.· ...... ~'::l"-:-:-:-:-:-:-:-:-::(7~?-!l ·=:=-=·=-=·=·=-=-r•:-:- 7 HH 48 A' 690.00, Legend • -••• --• -•••••• ••• ·--·· --· • ----• -----------·.· • • • • ---• • • -------• ---~-----------~ · · -----• _,_ _Ji• --------, Line of equal fluid potential (ft msl). Dashed • Inferred caprure zone Inner 1i w lls f:::::. --H~~i;~~;a-1 -S~;ie-i~· F~-~~-----·.-:::::::=:::::::::::::::::::::;::=;:;:;:;::=;::=;:;::::::::::=:::{:=:{::=::::;:;:!; ;:;::=;:;:;:;:;:::::~::\:::::::=::: ;'.;'.;:;'. ,I -810 where inferred. • • • -,er e •:•:-0 400 800 -:-:-:-:-:-:-:-:-•:•:;:-:-:-:-:-:•:•:•:•:-:-:-:-:-:-:-:-:-:-:-:-:-:-:-:-:-::::-:-:-:-:-:-:-:-:-:-:-:-:-:-:-c-:-H---·-·-:-•:-:-:-, :-:-: I ::: : : : : : : : : : : : : : : : : : : : : :: : :: :;: : : : : : : : :: : : : : :: : : : : : :: : :: : : :: :: : : : : :: : : :: :: : : : : ;:;: := :: : : j:::::::::::::::::::: =~-1 !:~!.! • •::::: :; Bedrock Potentiometric Surface Saprolite 850.00 -830.00 I I ] 810.00 ! l i J 790.00 I i ! 1 I 770.00 ' 750.00 730.00 1 710.00 l 690.00 ! I I i ! I j 670.00 Inferred direction of ground-water movement 0 000 Inferred capwre zone-Outer lier Wells Screened Interval of Well Kubal-Furr & Associates -En1>ironmental Consultants- Figure 4 -Hydrogeologic Cross-Section A-A' July II, 1996 Hoechst Celanese Corporation Shelby, North Carolina ., I' / -810 - 830.00 810.00 B 790.00 770.00 750.00 730.00 710.00 690.00 Line of equal fluid potential (ft msl). Dashed where inferred. Potentiometric Surface Inferred direction of ground-water movement ,.-.-,, ~ D Bedrock Saprolite Screened Interval of Well LAND SURFACE KubaJ ... Furr & Associates -. Environmental Consultants- B' 1 l I 1 I I J 830.00 810.00 790.00 770.00 750.00 730.00 710.00 690.00 670.00 Figure 5. Hydrogeologic Cross-Section B-B' July 11, 1996 Hoechst Celanese Corporation Shelby, North Carolina • Monitor well Water Level (ft msl) o Monitor Well Cluster A Plezometer Legend + Inner Tier Extraction Well (See Table for Water Levels) ♦ Outer Tier Extraction Well (See Table for Water Levels) + PEW Extraction Well 810 Stream/Creek m HCC Bulldlng/Structure / water-Level Contour 7f0 (Dashed where Inferred) ♦ Abandoned Outer Tier Well * Abandoned inner Tier Well a Domestic Supply Well ---===~=--<?0 '.::::::,--c:::=::--;-. ,,-,.<Ji'" ~ Kubal-Furr & Associates -Environmental Consultants- 0 Inner TI er W au:r Levels IT-I = 783.27 IT-2 ;: 775.95 IT-3 783.41 IT-4 784.15 IT-5 = 776.94 IT-6 782.00 IT-7 = 785.72 IT-8R = 795.22 IT-9 = <783.75 Outer Tier Water Levels OT-IR = 749.49 OT-2R = 723.36 OT-3 = 727 .58 OT-4 = 741.86 OT-5 = 726.82 OT-6 = 727.60 OT-6A = 719.60 OT-7 = 729.91 OT-7A = 77222 OT-8 = 756.99 OT-IO = 777.46 PEW W au:r Levels PEW-I = 765.80 PEW-3 = 809.37 PEW-4 = 766.18 i I --.. Sea le in Feet 400 800 Figure 6. Potentiometric Surface Map Shallow Saprolite -October 31, 1996 Hoechst Celanese Corporation Shelby, North Carolina • Monitor well 0 Monitor well cluster Legend + + Inner Tier Extraction Well ♦ Outer Tier Extraction Well c Domestic Supply Well ♦ PEW Extraction Well Plezometer Stream/Creek HCC BuDdlng/Structure Abandoned Outer Tier Well --'---,,_ ':.!':--c.s--w·: -~__,"' -.,.-:::=;,'==c:·-:::.: > -----------~ ,.::::, !.:-:.;~/--J " Abandoned Inner Tier Well A-A' Location of geologic cross-sections Kubal-Furr & Associates -Environmental Consultants- P0-58.•1 700.03 cm .. C I 0 Figure 7. Potentiometric Surface Map ---I I Scale In Feet 400 Deep Saprolite and Upper Bedrock-October 31, 1996 Hoechst Celanese Corporation Shelby, North Carolina 800 Plant Area 850.00, A ~---------r-- i 830.00 1 810.00 790.00 I 770.00 l ' 750.00 C i i ' l i I ! 730.00 ! [ ' ' ' i ' I 710.00 L r I i 690.00 L 0-27 (826.15) D-35 (825.96) 0-56 (825.78) Line of equal fluid potential (ft msl). Dashed where inferred. -Potentiomeaic S\Jrface Inferred direction of ground-water movement Inferred capwre zone-Outer lier Wells • • • • 810 Bedrock Saprolite G-50 (809.93) Screened Interval of Well • • J-28 (801.38) • • 800 790 Wastewarer Treatment Area----------------- 790 Kubal-Furr & Associates -Environmental Consultants- LAND SURfACE 850.00 -830.00 ' 810.00 790.00 770.00 A' 750.00 ' 730.00 : 710.00 0 690.00 -670.00 Figure 8. Hydrogeologic Cross-Section A-A' October 31, 1996 Hoechst Celanese Corporation Shelby, North Carolina I -810 .I I ,, - 830.00 810.00 B 790.00 770.00 750.00 730.00 [ 710.00 690.00 Pocentiometric Surface Inferred direction of ground-water movement Bedrock _· Saprolite LAND SURFACE Screened Inrerval of Well OT-4 Kubal-Furr & Associates -Environmental Consultants- 830.00 810.00. 790.00 770.00 l I I 1 I B' I I ! 750.00 7 I I i 730.00 710.00 j 690.00 670.00 fiaure 9. Hydrogeologic Cross-Section B-B' 0 October 31, 1996 Hoechst Celanese Corporation Shelby, North Carolina I I 11\NERTIER DAILY FLOW: I JULY 1996: IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9 I 07/01 /96 1 46 50 107 81 414 109 164 1 111 694 07/02/96 147 51 103 91 411 1 11 1 71 1126 705 07/03/96 144 49 106 90 407 107 170 1072 688 I 07/04/96 1 41 49 106 88 395 108 159 1057 679 07/05/96 141 51 104 88 400 106 164 1040 674 07/06/96 1 40 50 106 88 384 109 164 1044 674 07/07/96 139 50 1 1 8 88 389 11 0 165 1061 677 I 07/08/96 138 54 117 89 401 1 07 166 1053 667 07/09/96 135 52 112 90 406 1 04 1 61 1015 651 07/10/96 1 31 54 111 90 388 1 03 164 1017 652 07/11/96 134 54 106 85 375 100 163 986 658 I 07/12/96 1 38 56 79 18 387 102 165 1013 651 07/13/96 139 56 74 0 382 1 0 1 1 64 997 670 07/14/96 139 54 27 0 368 94 1 58 911 628 07/15/96 135 55 29 67 303 93 160 923 646 I 07/16/96 141 56 41 86 434 95 164 970 666 07/17/96 130 58 27 75 371 86 1 54 909 622 07/18/96 135 59 24 75 379 84 158 921 663 07/19/96 1 31 58 2 75 354 28 1 57 907 629 •• 07 /20/96 133 59 3 75 347 0 1 59 882 645 07/21/96 133 61 87 76 352 0 165 916 649 07/22/96 130 57 87 . 73 348 0 152 751 644 07/23/96 124 55 88 71 358 0 158 865 633 I 07/24/96 125 55 86 13 350 0 159 901 638 07/25/96 123 54 76 80 362 135 158 868 647 07/26/96 127 52 83 81 384 142 161 835 665 07/27/96 122 50 77 71 334 123 156 827 652 ·1 07/28/96 122 52 79 75 160 122 156 842 642 07/29/96 122 51 76 76 123 122 156 853 647 07/30/96 119 50 75 76 119 11 8 155 395 642 07/31/96 123 51 76 74 1 50 126 1 55 0 640 I ft VG: 133 54 77 71 346 89 1 61 905 656 I TOT: 4127 1663 2392 2205 10735 2745 4981 28068 20338 I .I I I I I I I CJUrER TIER DAILY FLOW: I JULY 1996: OT-1 OT-2 OT-3 OT-4 OT-5 OT-6 OT-6A OT-7 OT-8 07/01/96 26500 10100 2184 1356 1646 7826 9258 2713 18500 I 07/02/96 30500 3700 2052 1376 1837 7783 9303 2732 18400 07/03/96 30000 3700 1915 1365 1856 7642 9149 2694· 18000 07/04/96 29900 3900 1952 1339 1869 7642 9106 2691 17800 07/05/96 31300 1000 1968 1346 1865 7613 9112 2685 17800 I 07 /06/96 23800 5100 1984 1364 1845 7623 9245 2702 18000 07/07/96 22600 5600 1955 1367 1446 7581 9262 2708 18000 07/08/96 20000 10200 2252 1330 772 7390 8944 2620 17300 07/09/96 20700 10900 2347 1387 752 7743 9357 2751 18200 I 07/10/96 21300 10600 2292 1367 789 7513 9260 2622 15300 07/11/96 20900 1 0400 2232 1338 871 7337 9034 2603 16700 07/12/96 20900 1 0500 2266 1357 1334 7398 8996 2620 16800 07113/96 21400 1 0500 2298 1358 1383 7472 9100 2667 18200 I 07/14/96 21400 10600 2291 1361 1520 7496 9133 2687 17700 07/15/96 21700 10700 2295 1365 1544 7445 9062 2661 17500 07/16/96 21400 10600 2267 1 361 1464 7417 9092 2683 17500 07/17/96 21300 10500 2250 1334 1470 7301 8962 2652 17200 I 07/18/96 21400 1 0600 2265 1351 1522 7320 8975 2657 17200 07/19/96 21400 10600 2263 1357 1551 7347 8985 2646 17700 07/20/96 21700 10800 2278 1358 1674 7423 9079 2679 17900 07121/96 21800 10600 2292 1374 1744 7432 9136 27.04 18000 I 07/22/96 21500 11100 2241 1342 1715 7243 8941 1638 17600 07/23/96 21700 10900 2253 1 341 1712 7243 8944 2638 17400 07/24/96 22300 11100 2314 1391 1791 7537 9247 2713 18000 07/25/96 20700 10300 2167 1315 2021 7067 8692 2454 17700 I 07/26/96 21700 10700 2233 1354 2087 7341 9078 2508 1 8500 07/27/96 20100 10100 2155 1330 2128 6998 8583 2390 17800 07/28/96 20600 10400 2233 1 351 2359 7172 8819 2503 19100 07/29/96 21500 10800 1979 1331 2316 7306 9104 2500 19900 I G7/30/96 21300 10700 2131 1339 2388 7315 8992 2519 19700 07/31 /96 21300 10600 2225 1332 2323 7260 8998 2536 19700 AVG: 22729 9287 2188 1353 1664 7427 9063 2599 17906 •· TOT: 704600 287900 67829 41937 51594 230226 280948 80576 555100 I I I I I I I I I GROUNDWATER MONTHLY MONITORING: INNER TIER COMBINED INFLUENT #2 ITCI I PAGENO.1 JULY 1996 DATE: FLOW: PH: COD: TSS: TOC: I GD pH ppm ppm ppm 07/01/96 2876 5.4 5150 1 8 1323 I 07/02/96 2916 5.4 4750 6 07/03/96 2833 5.3 6070 1 0 07/04/96 2782 5.3 5950 7 I 07/05/96 2768 5.4 5090 7 07/06/96 2759 5.5 5110 9 07/07/96 2797 5.6 5010 1 0 I 07/08/96 2792 5.4 5260 9 07/09/96 2726 5.1 5010 1 8 1566 07/10/96 2710 5.3 4960 1 0 I 07/11/96 2661 5.4 5660 3 07/12/96 2609 5.3 5100 16 07/13/96 2583 5.3 4980 6 I 07/14/96 2379 5.3 5000 7 07/15/96 2411 5.4 5360 1 1 07/16/96 2653 5.5 5000 1 1 2110 I 07/17/96 2432 5.4 5000 1 4 07/18/96 2498 5.5 5370 1 6 07/19/96 2341 5.6 5140 1 1 I 07/20/96 2303 5.9 5330 1 3 07/21/96 2439 5.7 5410 1 0 07/22/96 2242 5.5 5510 1 0 I 07/23/96 2352 5.6 4840 1 0 1580 07/24/96 2327 5.5 5560 8 07/25/96 2503 5.4 5190 4 I 07/26/96 2530 5.4 4840 7 07/27/96 2412 5.5 4950 9 07/28/96 2250 5.5 5550 1 0 I 07/29/96 2226 5.6 5980 9 1885 07/30/96 1749 5.5 5670 9 .I 07/31/96 1395 5.3 6240 1 0 AVG: 2492 5.4 5292 1 0 1693 I MAX: 2916 5.9 6240 1 8 211 0 MIN: 1395 5.1 4750 3 1323 I I I I I GROUNDWATER MONTHLY MONITORING: OUTER TIER COMBINED INFLUENT: #1 OTCI I PAGENO.1 JULY 1996 DATE: FLOW: PH: TOC: I ffi) pH ppm 07/01/96 80083 5.9 1 8 I 07/02/96 77683 5.6 07/03/96 76321 6.8 07/04/96 76199 6.1 I 07/05/96 74689 6.0 07/06/96 71663 5.8 07/07/96 70519 5.5 I 07/08/96 70808 5.5 07/09/96 74137 6.0 4 07/10/96 71043 5.5 I 07/11/96 71415 6 .1 07/12/96 72171 6.2 07/13/96 74378 5.6 I 07/14/96 74188 5.7 07/15/96 74272 6.0 07/16/96 73784 5.9 6 I 07/17/96 72969 5.9 07/18/96 73290 5.8 07/19/96 73849 5.7 I 07/20/96 74891 5.6 07/21/96 75082 5.7 07/22/96 74320 5.9 I 07/23/96 74131 6.0 3 07/24/96 76393 5.9 07/25/96 72416 5.8 I 07/26/96 75501 5.7 07/27/96 71584 6. 1 07/28/96 74537 5.9 I 07/29/96 76736 5.7 8 07/30/96 76384 5.7 07/31 /96 76274 5.8 ,I AVG: 74249 5.9 8 I MAX: 80083 6.8 1 8 MIN: 70519 5.5 3 I I I I I GFOUNDWATER MONTHLY MONrrORING: SBR MIXED LIQUOR: SBRML PAGEN0.4 I JULY 1996 SETT. $LL.OGE 5/DAY DATE: PH: NH3N: P04: DO: MLSS: MLVSS: SOLIDS: WASTED F/M: F/M: pH ppm ppm ppm ppm ppm ml/I gal ratio ratio I 07/01/96 8.3 138 19.4 1.9 2400 150 148 0.18 07/02/96 8.0 124 35.0 1. 7 2764 170 135 0.14 07/03/96 8.4 131 18.9 1.8 4004 2000 170 120 0.10 I 07/04/96 8.3 168 28.0 1.6 2560 170 100 0.19 07/05/96 8.2 131 44.4 1.9 2884 190 100 0.13 0.15 07/06/96 8.1 114 32.8 1. 7 3000 160 108 0.13 0.14 0 710 7 /96 8.2 11 0 30.4 1.4 3440 170 100 0.12 0.13 I 07/08/96 8.3 168 33.0 1.6 ·3548 170 130 0.12 0.14 07/09/96 8.3 177 40.8 1.7 3288 170 150 0.13 0.13 07/10/96 8.4 147 35.6 1.8 2204 1440 160 202 0.20 0.14 07/11/96 8.2 140 22.1 1.9 3500 165 167 0.12 0.14 I 07/12/96 8.3 118 33.2 1.5 2024 150 175 0.18 0.15 07/13/96 8.3 125 32.0 1.9 2200 150 175 0.18 0.16 07/14/96 8.2 128 40.0 1.8 1884 140 135 0.19 0.17 07/15/96 8.4 160 24.0 1.6 1920 11 0 1 21 0.21 0.18 I 07/16/96 8.4 188 29.8 1.5 2204 110 142 0.18 0.19 07/17/96 .8.3 208 20.0 1. 7 2000 1300 120 135 0.22 0.19 07/18/96 8.2 198 19.9 1.6 2712 70 100 0.16 0.19 I 07/19/96 ·8.3 169 19.5 1.8 2320 70 60 0.18 0.19 07/20/96 8.4 160 20.0 1.7 2000 50 25 0.21 0.19 07/21/96 8.2 154 18.8 1.9 2268 50 54 0.19 0.19 07/22/96 8.5 220 16.4 1.6 1928 50 67 0.21 0.19 I 0 7 /23/96 8.6 202 23.9 1.6 1756 60 60 0.22 0.20 07/24/96 8.3 190 22.4 1.8 2040 1240 55 50 0.21 0.21 07/25/96 8.4 191 15.8 1.6 1760 65 40 0.21 0.21 07/26/96 8.3 211 25.5 1.4 1348 65 54 0.27 0.22 I 07/27/96 8.5 269 33.6 1.8 1644 70 54 0.26 0.23 07/28/96 8.5 256 32.0 1.5 1396 70 67 0.28 0.25 07/29/96 8.6 176 24.6 1.8 2264 55 54 0.20 0.24 0 7 /30/96 8.4 179 26.2 1. 7 1968 90 40 0.20 0.24 I 07/31/96 8.4 172 27.7 1.4 2048 1940 160 67 0.19 0.22 AVG: 8.3 168 27 2 2364 1584 116 101 0.18 0.18 I MAX: 8.6 269 44 2 4004 2000 190 202 0.28 0.25 MIN: 8.0 11 0 16 1348 1240 50 25 0.10 0.13 I I I I I I I I GROUNDWATER MONTHLY MONITORING: AFTER PLATE SEPARATOR BEFORE SBR: SBRI I PAGENO.3 ,JULY 1996 DATE: PH: COD: TSS: I pH ppm ppm 07/01/96 5.6 4750 24 I 07/02/96 5.8 4500 1 2 07/03/96 5.9 4630 40 07/04/96 5.6 5420 20 I 07/05/96 5.9 4320 24 07/06/96 6.0 4350 40 07/07/96 5.9 4550 36 I 07/08/96 5.9 4890 28 07/09/96 6.0 · 4720 44 07/10/96 6.0 4980 24 I 07/11/96 5.9 4790 28 07/12/96 6.1 4200 24 07/13/96 6.2 4350 24 I 07/14/96 5.9 4050 20 07/15/96 5.9 4500 1 6 07/16/96 6.3 4350 1 2 I 07/17/96 6.7 5000 1 6 07/18/96 6.6 4750 32 07/19/96 6.3 4610 24 I 07/20/96 6.4 4730 68 07/21 /96 6.6 4810 60 07/22/96 6.2 4610 68 I 07/23/96 6.1 4310 80 07/24/96 6.1 4730 64 07/25/96 6.1 4070 1 6 I 07/26/96 6.0 4170 24 07/27/96 6.2 4750 1 6 07/28/96 6.3 4450 24 I 07/29/96 6.2 5070 32 07/30/96 6.0 4430 40 I 07/31/96 6 .1 4270 48 AVG: 6.1 4584 33 I MAX: 6.7 5420 80 MIN: 5.6 4050 1 2 I I I I I GROUNDWATER MONTHLY MONITORING: SBR EFFLUENT:(DECANT) #4SBRE I PAGENO.5 JULY 1996 WAS. NH3N PHOS. DATE: FLOW: COD: TSS: TSS ADDED: ADDED: I GD ppm ppm ppm gal lbs 07/01/96 2159 525 230 9200 4 1 I 07/02/96 2188 500 168 10060 4 0 07/03/96 2359 510 80 13600 4 1 07/04/96 2485 507 96 11600 4 1 I 07/05/96 2330 478 108 8640 4 0 07/06/96 2328 446 84 9600 4 0 07/07/96 2375 479 120 10600 4 1 I 07/08/96 2267 542 292 12560 4 1 07/09/96 2215 351 216 11140 4 0 07/10/96 2226 500 80 10120 2 0 I 07/11/96 2297 574 148 13680 4 1 07/12/96 2311 580 200 11340 4 0 07/13/96 2333 540 200 11640 4 1 I 07/14/96 2192 520 220 111 00 4 0 07/15/96 2145 560 167 12360 4 1 07/16/96 2204 610 267 11920 2 1 I 07/17/96 2175 640 210 10400 2 1 07/18/96 2359 484 184 12980 2 1 07/19/96 2313 500 244 13440 2 1 I 07/20/96 2310 635 208 13500 4 1 07/21/96 2268 670 200 12140 4 1 07/22/96 2285 526 184 14780 2 1 •· 07/23/96 2275 390 192 13980 2 1 07/24/96 2268 614 204 13000 2 1 07/25/96 2276 534 225 12000 2 2 I 07/26/96 2288 534 160 8620 2 1 07/27/96 2216 600 184 9400 2 1 07/28/96 1905 610 188 9660 2 I 07/29/96 1 721 633 140 10240 2 1 07/30/96 2065 594 120 10880 2 1 I 07/31/96 2301 569 168 12000 2 1 AVG: 2240 540 177 11490 3 1 I MAX: 2485 670 292 14780 4 2 MIN: 1721 351 80 8620 2 0 I I I I I GROUNDWATER MONTHLY MONITORING: INNER TIER EQUALIZATION TANK: rTEQT I PAGENO.2 JULY 1996 DATE: PH: COD: OT WATER ADDED I pH ppm gal 07/01 /96 7.6 4800 I 07/02/96 7.4 4550 07/03/96 7.3 4840 07/04/96 7.3 5480 I 07/05/96 7.2 4890 07/06/96 7.3 4640 07/07/96 7.1 4610 I 07/08/96 7.3 4820 07/09/96 7.4 4880 07/10/96 7.4 4860 I 07/11 /96 7.3 4830 07/12/96 7.3 4500 07/13/96 7.3 4100 I 07/14/96 7.3 4400 07/15/96 7.8 4760 07/16/96 7.4 4800 I 07/17/96 7.3 4800 07/18/96 7.4 4710 450 07/19/96 7.5 4850 168 I 07/20/96 7.4 4950 242 07/21/96 7.5 4960 07/22/96 7.6 4930 319 I 07/23/96 7.8 4390 07/24/96 7.6 4880 400 07/25/96 7.7 4440 I 07/26/96 7.4 4210 07/27/96 7.8 4600 07/28/96 7.8 4700 I 07/29/96 7.7 6010 07/30/96 7.8 4810 400 07/31/96 7.7 3960 807 I AVG: 7.5 4741 398 I MAX: 7.8 6010 807 MIN: 7 .1 3960 168 I I I I I GROUNDWATER MONTHLY MONITORING: INNER TIER CARBON FILTER EFFWENT #8 ITEF I PAGE NO. 7 JULY 1996 DATE: PH: COD: TOC: TSS: I pH ppm ppm ppm 07/01 /96 I 07/02/96 07/03/96 8.3 442 22 07/04/96 I 07/05/96 07/06/96 07/07/96 I 07/08/96 07/09/96 142 07/10/96 8.3 530 I 07/11/96 07/12/96 07/13/96 I 07/14/96 07/15/96 07/16/96 35 I 07/17/96 8.4 610 07/18/96 07/19/96 I 07/20/96 07/21/96 07/22/96 I 07/23/96 312 07/24/96 8.5 552 07/25/96 I 07/26/96 07/27/96 07/28/96 I 07/29/96 401 07/30/96 07/31/96 8.2 295 I AVG: 8.3 486 222 22 I MAX: 8.5 610 401 22 MIN: 8.2 295 35 22 I I I I I GROUNDWATER MONTHLY MONITORING: OUTER TIER CARBON FILTER EFFLUENT: #7OTEF I PAGENO.3 JULY 1996 DATE: PH: TOG: TSS: I pH ppm ppm 07/01/96 I 07/02/96 07/03/96 8.5 4 07/04/96 I 07/05/96 07/06/96 07/07/96 I 07/08/96 07/09/96 3 07/1 0/96 7.1 I 07/11/96 07/12/96 07/13/96 I 07/14/96 07/15/96 07/16/96 7 I 07/17/96 7.3 07/18/96 07/19/96 I 07/20/96 07/21/96 07/22/96 I 07/23/96 2 07/24/96 7.2 I 07/25/96 07/26/96 07/27/96 I 07/28/96 07/29/96 6 07/30/96 I ,07/31/96 7.0 AVG: 7.4 4 4 I MAX: 8.5 7 4 MIN: 7.0 2 4 I I I I I GROUNDWATER MONTHLY MONrTORING: I RAINFALL DATA I DATE INCHES/DAY 07/01/96 0.00 I 07/02/96 0.00 07/03/96 0.00 07/04/96 0.00 I 07/05/96 0.00 07/06/96 0.00 07/07/96 0.00 I 07/08/96 0.10 07/09/96 0.10 I 07/10/96 0.00 07/11/96 0.00 07/12/96 0.00 I 07/13/96 0.10 07/14/96 0.00 07/15/96 0.60 I 07/16/96 0.00 07/17/96 0.00 07/18/96 0.00 I 07/19/96 0.00 07/20/96 0.00 07/21/96 0.00 I 07/22/96 0.00 07/23/96 0.00 07/24/96 0.00 I 07/25/96 0.00 07/26/96 1.00 07/27/96 0.00 I 07/28/96 0.00 07/29/96 0.00 07/30/96 0.00 I 07/31/96 0.40 TOTAL 2.30 I I I I I I I I I I I I I I I •· I I I I I I I MAINTENANCE ACTIVmESGRCXJNDWATER OPERABLE UNIT #1 NlER TIER SYSTEM DATE LOCATION NO MAINTENANCE REPOITTEDIN.IJLY ACTION DATE ACTION I I I I I I I I I I I I I I I I I I MAINTENANCE ACTIVmES-GROJNDWATER OPERABLE UNIT #1 OUTER 1ER SYSTEM DATE LOCATIC>N PRCH£M NO MAINTENANCE ACTIVITES REPOOlED IN JULY ACTKJN DATE ACTION MECH.ANC I I l~ERTIER DAILY FLOW: I i,UGUST I 1996: IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9 08/01/96 126 56 78 75 158 1 31 156 821 627 08/02/96 11 7 41 74 69 139 1 21 148 2 579 I 08/03/96 112 45 72 68 219 11 0 1 61 0 577 08/04/96 123 50 75 76 165 128 180 0 627 08/05/96 11 8 49 72 74 178 124 178 7 630 08/06/96 11 5 48 73 72 155 128 177 0 640 I 08/07/96 117 45 73 69 203 123 172 0 617 08/08/96 119 43 73 69 163 128 160 641 593 08/09/96 11 4 41 72 69 197 122 152 274 611 08/10/96 11 7 43 73 71 186 122 148 0 632 I 08/11 /96 113 40 70 70 315 117 123 0 592 08/12/96 11 3 41 69 69 313 11 8 112 0 615 08/13/96 117 42 68 69 299 114 108 781 624 08/14/96 1 1 7 44 70 69 171 114 111 753 613 I 08/15/96 105 38 60 62 142 90 142 976 9 08/16/96 125 42 74 74 248 113 187 805 581 08/17/96 11 2 39 66 64 140 114 172 727 616 08/18/96 1 11 35 64 61 349 1 07 1 55 685 579 I 08/19/96 83 33 67 62 3 51 109 164 738 610 08/20/96 82 34 65 61 348 1 08 165 748 614 08/21 /96 81 37 64 65 344 105 1 61 758 608 08/22/96 113 41 63 69 349 103 162 768 609 I 08/23/96 132 45 67 71 363 11 3 166 793 628 C 8/24/96 1 32 40 63 68 343 102 159 754 595 08/25/96 1 31 38 60 67 331 96 1 58 740 584 08/26/96 135 38 64 69 332 98 163 766 602 I 08/27/96 132 38 62 62 325 94 157 747 586 08/28/96 98 27 1 7 16 247 73 117 551 435 06/29/96 0 0 0 0 0 0 0 0 0 0~/30/96 0 0 0 0 0 0 0 0 0 I 08/31 /96 0 0 0 0 0 0 0 0 0 AVG: 104 37 60 60 228 1 0 1 1 39 446 524 I TOT: 3210 1153 1868 1860 7073 3125 4314 13835 16233 I I I I I I I I OUioRTIER DAILY FLOW: I Al-GUST 1996: OT-1 OT-2 OT-3 OT-4 OT-5 OT-6 OT-6A OT-7 OT-8 I 08/01 /96 21300 10700 2219 1346 2220 7257 9063 2522 19900 08/02/96 21500 10700 2156 1345 2234 7342 9133 2567 20100 08/03/96 21100 10500 2192 1302 2041 7121 8917 2522 19600 08/04/96 21400 10600 2243 1351 1966 7281 9086 2545 19900 I 08/05/96 21300 10500 2223 1323 1878 7148 8950 2487 19700 08/06/96 20300 10200 2183 1337 386 6863 8473 2499 1 8600 08/07/96 21600 10700 2139 1312 1208 7120· 8886 2547 19600 08/08/96 21600 10700 2116 1327 1362 7096 8809 2540 19300 I 08/09/96· 20600 10300 2093 1321 1285 6881 8466 2544 18500 08/10/96 21900 10700 2103 1334 1 341 7161 8864 2604 19300 08/11/96 21300 10600 2050 1325 1225 6978 8599 2582 18700 08/12/96 21000 1 0500 1913 1323 1259 6802 8457 2555 18400 I 08/13/96 21100 10600 1986 1317 1269 6958 8511 2600 18400 08/14/96 21300 10500 2014 1305 11 82 6994 8595 2587 18500 08/15/96 21300 10600 2027 1332 1186 7119 8676 2610 18500 08/16/96 21200 10600 2039 1318 1183 7040 8617 2629 18300 I 08/17/96 21700 10700 2014 1326 11 86 7119 8765 2599 18600 08/18/96 21700 10700 1917 1314 1186 7010 8792 2662 18500 08/19/96 21100 10400 1961 1308 11 so 6875 8594 2623 18100 08/20/96 21800 10800 1988 1310 1194 6919 8730 2639 18300 I 08/21/96 21900 10800 1981 1300 1132 6822 8668 2627 18000 08/22/96 22000 10800 1993 1 313 2468 6951 . 8699 2654 18200 08/23/96 22100 10900 2011 1327 2422 7111 8837 2716 18600 08/24/96 26958 10500 1940 1283 2391 6901 8471 2637 17900 I 08/25/96 21500 10700 1941 1289 2457 6826 8433 2637 17900 08/26/96 21300 10600 1956 1301 2520 7008 8580 2655 18200 08/27/96 22100 10700 1975 1301 2503 7097 8598 2650 18300 08/28/96 21400 10500 1961 1280 2437 6917 8488 2600 18000 I 08/29/96 21200 10400 1946 1263 2392 6702 8370 2543 17700 08/30/96 22200 10800 2035 1333 2569 7062 8781 2719 18500 08/31/96 20900 10500 1956 1279 2538 6843 8454 2621 17900 I /..VG: 21602 10606 2041 1314 1735 7010 8689 2597 18645 TOT: 669658 328800 63271 40745 53770 217324 269362 80522 578000 I I I I I I I I I GROUNDWATER MONTHLY MONITORING: INNER TIER COMBINED INFLUENT #2 ITCI I PAGENO.1 AUG.1996 DATE: FLOW: PH: COD: TSS: TOC: I cro pH ppm ppm ppm 08/01/96 2228 5.4 6100 8 I 08/02/96 1290 5.5 5840 9 08/03/96 1364 5.6 5790 1 0 08/04/96 1424 5.5 7410 7 I 08/05/96 1430 5.3 6850 8 08/06/96 1408 5.3 6430 1 3 1746 08/07/96 1419 5.4 7400 7 I 08/08/96 1989 5.3 6400 8 08/09/96 1652 5.4 5950 1 9 08/10/96 1392 5.4 7300 14 · I 08/11 /96 1440 5.3 6530 6 08/12/96 1450 5.4 6000 13 1714 08/13/96 2222 5.4 5500 8 I 08/14/96 2062 5.3 5570 10 08/15/96 1324 5.6 5510 6 08/16/96 2249 5.5 8450 4 I 08/17/96 2050 5.6 6110 1 0 08/18/96 2146 5.7 6240 9 08/19/96 2217 5.4 6070 1 8 I 08/20/96 2225 5.6 5940 7 1627 08/21/96 2223 5.5 5400 30 08/22/96 2277 5.6 5500 5 I 08/23/96 2378 5.4 5110 20 08/24/96 2256 5.4 5500 9 08/25/96 2205 5.4 5650 11 I 08/26/96 2267 5.4 5250 1 1 08/27/96 2207 5.5 5500 1 3 1752 08/28/96 1581 5.4 5450 1 0 I 08/29/96 S.B.R.DOWN FOR MAINT.,REPLACING DIFFUSERS 08/28/96 08/30/96 I 08/31/96 AVG: 1806 5.4 6098 11 171 0 I MAX: 2378 5.7 8450 30 1752 MIN: 0 5.3 5110 4 1627 I I I I I GROUNDWATER MONTHLY MONITORING: OUTER TIER COMBINED INFLUENT: #1 OTCI I PAGENO.1 AUG.1996 DATE: FLOW: PH: TOG: I (?f{) pH ppm 08/01 /96 76527 6.0 I 08/02/96 77077 6.1 . 08/03/96 75295 6.0 08/04/96 76372 5.5 I 08/05/96 75509 5.8 08/06/96 70841 5.7 5 08/07/96 73904 6.0 I 08/08/96 74850 6.1 08/09/96 71190 6.1 08/10/96 75307 6.1 I 08/11 /96 73359 5.9 08/12/96 72209 6.0 5 08/13/96 72741 6.2 I 0 8/1 4/96 72977 5.3 08/15/96 73350 6.1 08/16/96 72926 6.0 -I 08/17/96 74009 5.8 08/18/96 73781 5.6 I 08/19/96 72111 6.7 08/20/96 73680 6.4 3 08/21/96 73230 5.4 I 08/22/96 75078 6.9 08/23/96 76024 6.2 08/24/96 73623 6.3 I 0 8/25 /9 6 73683 6.3 08/26/96 74120 6.5 08/27/96 75224 6.6 3 I 08/28/96 73583 6.5 08/29/96 08/30/96 I 08/31/96 AVG: 74021 6.1 4 I MAX: 77077 6.9 5 MIN: 70841 5.3 3 I I I I I GOOUNDWATER MON™LY MONITORING: SBA MIXED LIQUOR: SBRML PAGEN0.4 I AUG.1996 SETT. SlUlGE 5/DAY DATE: PH: NH3N: P04: DO: MLSS: MLVSS: SOLIDS: WASTED F/M: F/M: pH ppm ppm ppm ppm ppm ml/I gal ratio ratio I 08/01/96 8.6 180 24.0 1.6 2092 180 20 0.00 08/02/96 8.5 213 25.1 1.6 2160 185 80 0.22 08/03/96 8.6 200 24.0 1.9 2320 180 54 0.20 I 08/04/96 8.7 194 22.4 1.6 2160 180 54 0.20 08/05/96 8.6 210 28.9 1.6 1964 180 0 0.00 0.12 08/06/96 8.5 218 43.2 1. 7 2088 200 81 0.20 0.16 08/07/96 8.4 222 30.8 1.8 1820 1160 240 0 0.00 0.12 I 08/08/96 8.5 216 30.0 1. 7 1800 210 81 0.26 0.13 08/09/96 8.4 219 40.0 1.4 1520 300 81 0.31 0.15 08/10/96 8.3 215 28.0 1.3 1760 450 0 0.00 0.15 08/11/96 8.4 210 34.0 1.8 1584 350 108 0.30 0.17 I 08/12/96 8.4 232 35.2 1.7 1724 400 154 0.28 0.23 08/13/96 8.4 230 25.9 1.5 1960 625 154 0.23 0.22 08/14/96 8.3 204 22.4 1.3 2228 1724 550 130 0.18 0.20 08/15/96 8.5 206 38.3 1.5 1696 550 194 0.24 0.25 I 08/16/96 8.4 246 30.2 1.9 2192 600 135 0.16 0.22 08/17/96 8.3 210 28.0 1.8 2080 575 148 0.16 0.19 08/18/96 8.2 205 27.8 1. 7 2120 615 175 0.17 0.18 08/19/96 8.4 217 22.2 1.4 2184 550 148 0.15 0.17 I 08/20/96 8.3 156 17.9 1.7 1844 550 165 0.23 0.17 08/21/96 8.2 164 20.8 1.8 2124 1448 600 135 0.18 0.18 08/22/96 8.3 178 33.9 1.6 1984 625 1 21 0.22 0.19 I 08/23/96 8.3 173 32.0 1.4 1704 600 1 21 0.21 0.20 08/24/96 8.3 226 40.0 1.5 1900 950 135 0.21 0.21 08/25/96 8.4 219 40.0 1.4 1804 800 135 0.22 0.21 08/26/96 8.5 192 29.2 1.5 1888 900 94 0.19 0.21 I 08/27/96 8.4 173 21.6 1.6 1824 900 105 0.21 0.21 08/28/96 8.4 123 12.0 1.3 1840 1304 900 0.00 0.17 08/29/96 08/30/96 I 08/31 /96 AVG: 8.4 202 29 2 1942 1409 498 104 0.18 0.18 MAX: 8.7 246 43 2 2320 1724 950 194 0.31 0.25 I MIN: 8.2 123 1 2 1520 1160 180 0 0.00 0.12 I I I I I I I I GROUNDWATER MONTHLY MONITORING: AFTER PLATE SEPARATOR BEFORE SBR: SBRI I PAGENO.3 AUG.1996 DATE: PH: COD: TSS: I pH ppm ppm 08/01/96 I 0 8/0 2/9 6 6.0 5260 20 08/03/96 6.1 5310 32 08/04/96 6.0 4810 40 I 08/05/96 08/06/96 6.2 4810 56 08/07/96 I 08/08/96 5.7 5300 24 08/09/96 5.5 5300 1 6 08/1 0/96 I 08/11 /96 6.2 5370 1 2 08/12/96 5.9 5500 1 6 08/13/96 6.1 5000 28 I 08/14/96 6.2 4590 24 08/15/96 6.6 4490 32 08/16/96 6.2 3850 96 I 08/17/96 5.9 3810 44 08/18/96 6.1 3940 40 08/19/96 6.0 3590 48 I 08/20/96 6.2 4710 48 08/21 /96 5.8 4350 24 I 08/22/96 5.9 5010 20 0 8/23/9 6 5.9 4070 68 08/24/96 6.0 4400 1 6 I 08/25/96 6.1 4550 28 08/26/96 5.7 4100 28 08/27/96 5.7 4350 20 I 08/28/96 08/29/96 08/30/96 I 08/31/96 AVG: 4629 34 6.0 I MAX: 6.6 5500 96 MIN: 5.5 3590 1 2 I I I I I GROUNDWATER MONTHLY MONITORING: SBR EFFLUENT:(DECANT) #4SBRE I PAGENO.5 AUG.1996 WAS. NH3N PHOS. DATE: FLOW: COD: TSS: TSS ADDED: ADDED: I GPO ppm ppm ppm gal lbs 08/01/96 600 204 11000 2 1 I 0 8/02/9 6 2000 564 260 11840 0 1 08/03/96 2292 570 240 12000 2 1 08/04/96 2177 622 200 11 000 0 1 I 0 8/0 5/9 6 1 08/06/96 2213 390 188 10200 1 0 08/07/96 1 1 I 08/08/96 2205 360 140 9800 1 1 08/09/96 2303 405 160 6520 1 1 08/10/96 1 1 I 08/11 /96 2183 470 240 8080 1 0 08/12/96 2271 510 246 7240 1 1 08/13/96 2152 460 180 7800 0 1 I 08/14/96 2082 404 140 4000 0 1 08/15/96 2096 400 148 11200 0 0 08/16/96 2273 330 144 9800 0 0 I 08/17/96 2172 596 160 10200 3 1 08/18/96 2341 480 200 12000 3 1 08/19/96 2322 440 256 9640 0 1 I 08/20/96 2280 364 272 5480 1 1 08/21/96 2329 330 160 5680 1 1 08/22/96 2212 300 160 6640 1 1 I 0 8/23/9 6 2218 320 88 12560 1 1 08/24/96 2240 290 1 04 7200 1 1 08/25/96 2203 285 132 5480 1 1 I 08/26/96 2228 240 128 5420 1 1 08/27/96 2262 250 92 6580 0 0 08/28/96 I 08/29/96 08/30/96 08/31/96 I AVG: 2220 416 177 8640 1 1 MAX: 2341 622 272 12560 3 1 I . MIN: 2000 240 88 4000 0 0 I I I I I GROUNDWATER MONTHLY MONITORING: INNER TIER EQUALIZATION TANK: ITEQT ,I PAGENO.2 AUG.1996 DATE: PH: COD: OT WATER ADDED I pH ppm gal 08/01/96 7.9 5000 I 08/02/96 7.8 5360 08/03/96 7.7 5420 08/04/96 7.8 4820 I 08/05/96 7.9 4700 08/06/96 7.8 4660 08/07/96 8.1 5150 I 08/08/96 7.9 5250 08/09/96 7.4 5300 08/1 0/96 7.5 4850 I 08/11/96 7.4. 5770 08/12/96 7.5 5450 678 08/13/96 7.5 5300 650 I 08/14/96 7.4 4730 440 08/15/96 7.6 4650 502 08/16/96 7.5 3910 200 I 08/17/96 7.4 4020 08/18/96 7.5 4110 08/19/96 7.3 4010 400 I 08/20/96 7.3 4950 285 08/21/96 7.4 4700 408 08/22/96 7.3 5140 530 I 0 8/23/9 6 7.4 4780 304 08/24/96 7.6 4650 400 0 8/2 5/9 6 7.6 4850 375 I 08/26/96 7.7 4200 209 08/27/96 7.4 4100 08/28/96 7.4 4450 I · 08/29/96 08/30/96 08/31/96 I AVG: 7.6 4796 414 MAX: 8.1 5770 678 I MIN: 7.3 3910 200 I I I I I GROUNDWATER MONTHLY MONITORING: INNER TIER CARBON FILTER EFFWENT I PAGE NO. 7 AUG.1996 DATE: PH: COD: TOC: TSS: I pH ppm ppm ppm 08/01/96 I 08/02/96 08/03/96 08/04/96 I 08/05/96 08/06/96 124 08/07/96 8.4 310 66 I 08/08/96 08/09/96 08/10/96 I 08/11/96 08/12/96 08/13/96 36 I 08/14/96 8.5 425 08/15/96 08/16/96 I 08/17/96 08/18/96 08/19/96 I 08/20/96 52 08/21 /96 8.3 305 08/22/96 I 08/23/96 08/24/96 08/25/96 I 08/26/96 08/27/96 107 08/28/96 I 08/29/96 08/30/96 08/31/96 I AVG: 8.4 347 80 66 MAX: 8.5 425 124 66 I MIN: 8.3 305 36 66 I I I I I GROUNDWATER MONTHLY MONITORING: OUTER TIER CARBON FILTER EFFLUENT: #7OTEF I PAGENO.3 AUG.1996 DATE: PH: TOG: TSS: I pH ppm ppm 08/01 /96 I 08/02/96 08/03/96 08/04/96 I 08/05/96 08/06/96 3 08/07/96 7.0 4 I 08/08/96 08/09/96 . 08/10/96 I 08/11 /96 08/12/96 08/13/96 3 I 08/14/96 7.4 08/15/96 08/16/96 I 08/17/96 08/18/96 08/19/96 I 08/20/96 2 08/21/96 7.5 08/22/96 I 08/23/96 08/24/96. 0 8/25/9 6 I 08/26/96 08/27 /96 3 08/28/96 I 08/29/96 08/30/96 •• 08/31/96 AVG: 7.3 3 4 I MAX: 7.5 3 4 MIN: 7.0 2 4 I I I n m GROUNDWATER MONTHLY MONrTOF I RAINFALL DATA I DATE INCHES/DAY 08/01 /96 0.00 I 08/02/9 6 0.00 0 8/03/9 6 0.30 08/04/96 0.00 I 08/05/96 0.40 08/06/96 0.00 08/07/96 0.1 0 :I 08/08/96 0.00 08/09/96 0.00 08/10/96 0.00 I 08/11/96 0.60 08/1 2/96 0.90 08/13/96 0.20 I 08/14/96 0.00 08/15/96 0.00 08/16/96 0.00 I 08/17/96 0.00 08/18/96 0.00 08/19/96 0.00 1· 08/20/96 0.00 08/21/96 0.00 08/22/96 0.00 •• 0 8/23/9 6 0.00 08/24/96 0.00 08/25/96 0.00 I 08/26/96 0.20 08/27/96 0.50 08/28/96 0.20 I 08/29/96 0.00 08/30/96 0.00 I 08/31/96 0.00 TOTAL 3.40 I ,I I I D MAINTENANCE ACTIVmES-GROUNDWATER OPERABLE UNIT #1 I l~ERTIERSYSTEM I I I I I I I I •· I I I I I I DATE 07126196 08112196 08114196 08116196 08110196 08122196 08128196 LOCATION IT-1 IT-8 IT-7 IT-9 IT-2 IT-4 S.B.R. ACTION PR)8l£M DATE LOW FLOW 08121196 LOW FLOW 08112196 LOW FLOW 08114196 NO FLOW 08116196 LOW FLOW 08121196 LOW FLOW 08122196 RUPTU1ED DIFFUSER 08128196 ACTION REPLACED BLADDER REPLACED AIR REGULATOR REPLACED BLADDER CLEANED PROBES REPLACED BLADDER REPLACED AMPUFIER f,/()!)ULE DRAINED S.B.R. TO REPLACE DIFFUSERS MECHMIIC Fl' Fl' Fl' Fl' Fl' Fl' PP.P D fl MAINTENANCE ACTIVmEs-GROJNOWATER OPERABlE UNIT #1 OUTm TEA SYSTEM I I I I I I I I I I I I I I I I I DATE LOCATION 08/22/96 OT-5 PRC8..EM LOW FLOW ACTION DATE 08/22/96 ACTION CHANGED PUMP & RESET FLOW RATE MECHANC PPPWBH 0 I li'i'JER llER DAILY FLOW: I SEFT. 1996: IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9 I 09/01 /96 0 0 0 0 0 0 0 0 0 09/02/96 0 0 0 0 0 0 0 0 0 09/03/96 0 0 0 0 0 0 0 0 0 I 09/04/96 0 0 0 0 0 0 0 0 0 09/05/96 0 0 0 0 ·O 0 0 0 0 09/06/96 124 53 83 65 297 82 138 135 0 09/07/96 144 58 71 66 362 106 184 493 0 I 09/08/96 128 56 62 55 307 97 164 706 0 09/09/96 134 43 65 56 323 106 174 848 0 09/10/96 128 32 56 53 329 104 172 900 569 09/11 /96 137 38 63 48 348 87 168 875 631 I 09/12/96 131 37 58 53 336 1 02 161 875 608 09/13/96 128 34 56 50 319 95 1 58 737 597 09/14/96 129 38 66 54 338 99 159 744 601 09/15/96 1 21 37 65 54 333 97 155 708 587 I 09/16/96 130 38 67 45 326. 100 155 718 601 09/17/96 130 31 65 0 322 98 156 710 607 09/1 8/96 122 34 63 0 315 98 157 722 618 09/19/96 99 30 52 28 255 81 130 602 520 I 09/20/96 106 44 66 49 187 89 140 707 566 09/21 /96 92 43 68 54 174 97 162 752 635 0 9/22/96 94 44 66 53 171 97 1 58 737 919 09/23/96 85 41 56 46 202 85 1 37 649 542 I 09/24/96 88 34 63 47 290 99 135 8 546 09/25/96 96 34 63 51 347 104 164 0 626 09/26/96 1 00 39 60 50 351 100 160 408 621 09/27/96 88 42 58 47 289 96 118 563 572 I 09/28/96 94 44 64 51 195 105 31 581 615 09/29/96 88 45 63 50 128 104 26 585 616 09/30/96 69 48 63 64 282 108 23 589 604 I AVG: 93 34 53 40 238 81 116 512 427 I TOT: 2785 1017 1582 1189 7126 2436 3485 15352 12801 I •• I I I I g I OIJTERTIER DAILY FLOW: I SEPT. 1996: OT-1 OT-2 OT-3 OT-4 OT-5 OT-6 OT-6A OT-7 OT-8 09/01/96 22300 10600 1931 1268 2588 6839 8369 2573 17600 I 09/02/96 21500 10800 1853 1278 2778 6779 8359 2577 17700 09/03/96 22200 10900 1884 1302 2927 6970 8662 2617 18400 09/04/96 21300 10400 1980 1260 2700 6742 8389 2537 17700 09/05/96 21600 10500 2013 1285 2664 6696 8536 2588 17900 I 09/06/96 21800 10600 2008 1295 2685 6778 8595 2632 18100 09/07/96 21700 10600 1987 1281 2657 6745 8510 2593 17800 09/08/96 -21600 10600 1966 1267 2657 6674 8437 2584 17600 09/09/96 21700 10500 1956 1268 2675 6667 8431 2570 17600 I 09/10/96 21300 10300 1925 1251 2642 6610 8298 2535 17200 09/11/96 21700 1 0500 1974 1272 2731 6767 8474 2586 17600 09/12/96 21600 10400 1966 1271 2735 6852 8414 2542 17400 09/13/96 21200 10300 1922 1241 2714 6757 8267 2459 17100 I 09/14/96 22000 10600 1997 1284 2807 6941 8520 4513 17700 09/15/96 21300 10300 1924 1229 2718 6438 8234 431 17100 09/16/96 21400 10200 1945 1248 2795 6311 8358 2522 17100 09/17/96 21400 10200 1953 1256 2856 6348 8341 2508 17100 I 09/18/96 21600 10400 1989 1255 2928 6659 8427 2524 17400 09/19/96 22100 10600 2021 1269 2989 6908 8590 2554 17900 09/20/96 21400 10200 1963 1241 2907 6634 8085 2504 17300 09/21 /96 21600 10200 1967 1247 2939 6484 8173 2557 17400 I 09/22/96 21400 1 0200 1972 1240 2949 6536 8205 2500 17400 09/23/96. 21300 9800 1876 1238 2956 6631 8339 2526 17600 09/24/96 21400 9800 1876 1256 3011 6467 8442 2539 17900 09/25/96 21700 10000 1865 1252 3061 6380 8446 2587 18000 I 09/26/96 21100 9600 1830 1219 3034 6160 7854 2535 17400 09/27/96 21500 9900 1919 1257 3097 6329 6597 2607 17800 09/28/96 21200 9700 1977 1232 3074 6316 7262 2563 17500 09/29/96 21200 9700 1985 1246 3066 6602 6643 2572 17600 I 09/30/96 21300 9700 2017 1245 3078 6813 6103 2580 17700 AVG: 21547 10270 1948 1258 2847 6628 8145 2551 17587 •· TOT: 646400 308100 58441 37753 85418 198833 · 244360 76515 527600 I I I I I I I u I GROUNDWATER MONTHLY MONITORING: INNER TIER COMBINED INFLUENT #2 ITCI I PAGENO.1 SEPT 1996 DATE: FLOW: PH: COD: TSS: TOC: I GPO pH ppm ppm ppm 09/01 /96 I 09/02/96 09/03/96 09/04/96 I 09/05/96 09/06/96 977 09/07/96 1484 I 09/08/96 1575 09/09/96 1749 09/10/96 2343 I 09/11/96 2395 09/12/96 2361 09/13/96 2174 I 09/14/96 2228 09/15/96 2157 09/16/96 2180 I 09/17/96 211 9 09/18/96 2129 09/19/96 1797 . 5.5 5460 1 0 I 09/20/96 1954 5.5 5500 7 09/21 /96 2077 5.5 5050 7 09/22/96 2039 5.4 5550 6 .I 09/23/96 1843 5.5 5350 1 0 09/24/96 1310 5.5 4500 7 2302 I 09/25/96 1485 5.5 4970 1 5 09/26/96 1889 5.5 5350 5 09/27/96 1873 5.6 4840 3 I 09/28/96 1780 5.5 3960 3 09/29/96 1705 5.4 5050 5 09/30/96 1850 5.6 5610 1 5 I AVG: 1899 5.5 5099 8 2302 I MAX: 2395 5.6 5610 1 5 2302 MIN: 977 5.4 3960 3 2302 I I I I I GROUNDWATER MONTHLY MONrrORING: OUTER TIER COMBINED INFLUENrr: #1 OTCI I PAGENO.1 SEPT 1996 DATE: FLOW: PH: TOC: I ffi) pH ppm 09/01/96 74068 6.0 I 09/02/96 73624 6.3 09/03/96 75862 5.9 09/04/96 73008 6.1 I 09/05/96 73782 5.9 09/06/96 74493 6.8 09/07/96 73873 6.0 I 09/08/96 73385 6.7 09/09/96 73367 5.9 09/10/96 72061 6.0 I 09/11/96 73604 6.0 09/12/96 73180 6.2 09/13/96 71960 6. 1 I 09/14/96 76362 6.2 09/15/96 69674 6.0 09/16/96 71879 6.0 I 09/17/96 71962 5.8 09/18/96 73182 5.9 09/19/96 74931 6.0 I 09/20/96 72234 6.0 09/21/96 72567 6.0 09/22/96 72402 6.0 I 09/23/96 72266 6.1 09/24/96 72691 6.0 9 I 09/25/96 73291 6.0 09/26/96 70732 6.0 09/27/96 71006 6. 1 I 09/28/96 70824 6.0 09/29/96 70614 6.1 09/30/96 70536 6.3 I AVG: 72781 6.1 9 I MAX: 76362 6.8 9 MIN: 69674 5.8 9 I I I I I GFOUNDWATEA MONTHLY MONITORING: SBA MIXED LIOLOR: SBRML PAGEN0.4 I SEPT 1996 SETT. Sl.l.OGE 5/DAY DATE: PH: NH3N: P04: DO: MLSS: MLVSS: SOLIDS: WASTED F/M: F/M: pH ppm ppm ppm ppm ppm mill gal ratio ratio I 09/01/96 09/02/96 09103/96 I 09/04196 09/05/96 0.00 09/06/96 0.00 09/07/96 0.00 I 09108/96 0.00 09/09/96 0.00 09/10/96 0.00 09/11/96 0.00 I 09/12/96 0.00 09/13/96 0.00 09/14/96 0.00 09/15/96 0.00 I 0911 6/96 0.00 09/17/96 0.00 09/18/96 0.00 I 09/19/96 8.3 116 57.2 1.9 908 0.00 09120/96 8.4 142 52.0 1. 7 900 0.00 09/21/96 8.3 139 48.0 2.0 1248 0 0.35 0.07 09/22/96 8.3 141 40.0 1.8 1164 40 0 0.39 0.15 I 09/23/96 8.2 158 56.0 1. 7 404 50 0 0.00 0.15 09124/96 8.4 203 66.4 1.9 840 50 0 0.51 0.25 09/25196 8.3 181 40.0 1.9 496 404 35 0 0.90 0.43 09126/96 8.3 195 50.8 1.9 · 1104 60 0 0.00 0.36 I 09/27/96 8.2 185 60.8 1.8 880 70 0 0.46 0.37 09/28/96 8.1 180 50.4 1.9 1332 70 0 0.28 0.43 09/29/96 8.0 184 48.4 1.7 1380 80-0 0.36 0.40 09/30/96 8.2 170 24.4 1.9 1224 90 0 0.00 0.22 I AVG: 8.3 166 50 2 990 404 61 0 0.32 0.11 MAX: 8.4 203 66 2 1380 404 90 0 0.90 0.43 I MIN: 8.0 11 6 24 2 404 404 35 0 0.00 0.00 I I I I I I I I GROUNDWATER MONTHLY MONITORING: AFTER PLATE SEPARATOR BEFORE SBR: SBRI I PAGENO.3 SEPT 1996 DATE: PH: COD: TSS: I pH ppm ppm 09/01/96 I 09/02/96 09/03/96 09/04/96 I 09/05/96 09/06/96 09/07 /96 I 09/08/96 09/09/96 09/10/96 I 09/1.1 /96 09/12/96 09/13/96 I 09/14/96 09/15/96 09/16/96 I 09/17/96 09/18/96 09/19/96 I 09/20/96 6.0 6300 32 09/21 /96 6.0 4950 1 6 09/22/96 5.7 5100 1 2 I 09/23/96 09/24/96 5.5 4800 1 6 09/25/96 5.6 5030 52 I 0 9/2 6/9 6 09/27/96 5.9 4520 68 I 09/28/96 5.6 4260 1 6 09/29/96 5.7 5520 24 09/30/96 I AVG: 5.8 5060 30 I MAX: 6.0 6300 68 MIN: 5.5 4260 1 2 I I I I I GROUNDWATER MONTHLY MONITORING: SBR EFFLUENT:(DECANT) #4SBRE I PAGENO.5 SEPT 1996 WAS. NH3N PHOS. DATE: FLOW: COD: TSS: TSS ADDED: ADDED: I CR) ppm ppm ppm gal lbs 09/01/96 I 0 9/0 2/9 6 09/03/96 09/04/96 I 09/05/96 09/06/96 09/07/96 I 09/08/96 09/09/96 09/10/96 I 09/11/96 09/12/96 09/13/96 I 09/14/96 09/15/96 09/16/96 I 09/17/96 09/18/96 09/19/96 1035 333 I 09/20/96 2455 545 250 09/21 /96 2494 390 200 1 0 09/22/96 2164 285 166 1 0 I 09/23/96 1 1 09/24/96 1560 290 199 1 0 I 09/25/96 2489 270 52 1 0 09/26/96 0 245 84 0 0 09/27/96 2289 212 68 0 0 I 09/28/96 2448 197 20 0 0 09/29/96 1 91 6 212 80 1 0 09/30/96 0 206 84 0 1 I AVG: 1782 353 140 0 1 0 I MAX: 2494 1035 333 0 1 1 MIN: 0 197 20 0 0 0 I I I m I GROUNDWATER MONTHLY MONrTORING: INNER TIER EQUALIZATION TANK: rTEOT I PAGENO.2 SEPT 1996 DATE: PH: COD: OT WATER ADDED I pH ppm gal 09/01/96 I 09/02/96 09/03/96 09/04/96 I 09/05/96 09/06/96 09/07/96 I 09/08/96 09/09/96 09/10/96 I 09/11/96 09/12/96 09/13/96 I 09/14/96 09/15/96 09/1 6/96 I 09/17/96 09/1 8/96 09/19/96 7.6 5100 I 09/20/96 7.1 5100 09/21 /96 7.1 4450 09/22/96 7.3 5000 I 09/23/96 7.3 5100 09/24/96 7.2 4850 345 I 09/25/96 7 .1 4880 0 9/26/9 6 7.5 4250 09/27/96 7.5 4520 I 09/28/96 7.3 4810 09/29/96 7.2 5420 09/30/96 7.4 4580 I AVG: 7.3 4838 345 I MAX: 7.6 5420 345 MIN: 7.1 4250 345 I I I u m GROUNDWATER MONTHLY MONITORING: INNER TIER CARBON FILTER EFFWENT #8 ITEF I PAGE NO. 7 SEPT 1996 DATE: PH: COD: TOC: TSS: I pH ppm ppm ppm 09/01 /96 I 09/02/96 09/03/96 09/04/96 I 09/05/96 09/06/96 09/07/96 I 09/08/96 09/09/96 09/10/96 I 09/11 /96 09/12/96 09/13/96 I 09/14/96 09/15/96 09/16/96 I 09/17/96 09/18/96 09/19/96 I 09/20/96 09/21/96 09/22/96 I 09/23/96 09/24/96 80 I 09/25/96 8.3 263 09/26/96 09/27/96 I 09/28/96 09/29/96 09/30/96 I AVG: 8.3 263 80 0 I MAX:· 8.3 263 80 0 MIN: 8.3 263 80 0 I I I 0 I GROUNDWATER MONTHLY MONITORING: I OUTER TIER CARBON FILTER EFFLUENT: #7 OTEF PAGENO.3 SEPT 1996 I DATE: PH: TOC: TSS: pH ppm ppm I 09/01 /96 09/02/96 09/03/96 I 09/04/96 7 .1 5 09/05/96 09/06/96 I 09/07/96 09/08/96 09/09/96 I 09/10/96 09/11/96 09/12/96 I 09/13/96 09/14/96 09/15/96 I 09/16/96 09/17/96 09/18/96 I 09/19/96 09/20/96 09/21 /96 I 09/22/96 09/23/96 09/24/96 6 I 0 9/25/9 6 6.7 09/26/96 09/27/96 I 09/28/96 09/29/96 09/30/96 I AVG: 6.9 6 5 I MAX: 7 .1 6 5 . MIN: 6.7 6 5 I I I g I GROUNDWATER MONTHLY MONITOF I RAINFALL DATA I DATE INCHES/DAY 09/01 /96 0.00 I 09/02/96 0.00 09/03/96 1 .1 0 09/04/96 0.00 I 09/05/96 0.00 09/06/96 0.00 09/07/96 0.00 I 09/08/96 0.00 09/09/96 0.00 09/10/96 0.00 ·I 09/11/96 0.00 09/12/96 0.00 09/13/96 0.00 I 09/14/96 0.00 09/15/96 0.00 09/16/96 1.60 I 09/17/96 0.00 09/18/96 0.00 09/19/96 0.00 I 09/20/96 0.00 09/21 /96 0.20 I 09/22/96 0.00 09/23/96 0.00 09/24/96 0.00 I 09/25/96 0.00 09/26/96 0.00 09/27/96 0.00 I 09/28/96 0.90 09/29/96 0.00 09/30/96 1.50 I TOTAL 5.30 I I I I I I I I I I I I I I •· I I I I I I I MAINTENANCE ACTIVmESGROUNDWATER OPERABLE UNIT #1 NNER TIER SYSTEM DATE LOCATION PR:B.EM 09/06/96 CAUlTIC PUMP NOTPUMPNG 09/09/96 IT-6 LOW FLOW 09/09/96 IT-9 LOW FLOW 09/16/96 IT-6 LOW FLOW 09/20/96 IT-1 LOW FLOW 09/22/96 IT-5 LOW FLOW 09/25/96 IT-6 NO FLOW ACTION DATE ACTION MECHANIC 09/06/96 REPLACED DIAPHRAIM & CHECK VALVE JPPP 09/11 /96 REPLACED TIMMER JPPP 09/1 0/96 REPLACED PUMP JPPP 09/23/96 REPLACED BlADDER CLEANED SCREEN JPPP 09/20/96 REPAIRED BROKEN UNE JPPP 09/23/96 REPLACED BlADDER CLEANED SCREEN ADJUSTED FLOW JPPP 09/26/96 REPLACED PUMP.REGULATOR & PRESSURE GUAGE & CLEANED LINE JPPP I I I I I I I I I I I I I I I I I I I MAINTENANCE ACTIVITIES{;ROUNDWATER OPERABI.E UNIT #1 OUTER TIER SYSTEM DATE LOCATION 09/16/96 OT-7 PACaEM LOW FLOW ACTION DATE 09/16/96 ACTION ADJUSTED FLOW MECH#JIC JPPP I I INNER TIER DAILY FLOW: I OCT. I 1996: IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9 10/01/96 65 39 61 1 5 118 108 136 503 545 1 0/02/96 118 44 55 35 311 1 21 162 535 642 I 1 0/03/96 11 4 43 53 25 333 11 6 1 49 463 629 1 0/04/96 104 44 53 33 165 119 143 424 645 1 0105196 94 42 50 28 129 103 125 567 568 1 0106196 126 46 55 34 0 117 153 574 664 I 10107196 133 44 53 33 243 118 1 41 523 636 10108196 116 39 50 47 331 128 135 507 610 1 0109/96 98 41 50 54 349 128 145 71 649 10/10196 1 02 41 51 59 361 125 139 0 656 I 10111/96 100 47 56 63 415 134 148 0 723 -0112196 83 3.8 46 44 353 11 3 125 0 621 10113/96 91 40 50 28 369 11 8 135 0 668 10/14/96 11 0 42 51 41 339 11 7 135 0 668 I 1 0115196 1 00 45 50 55 347 1 19 138 0 679 10116196 106 46 48 67 332 11 5 134 0 662 10117/96 11 3 48 50 64 331 114 137 0 668 10118/96 94 49 51 55 334 114 140 0 677 I 10119/96 94 46 49 42 325 11 0 135 0 650 1 0120/96 79 48 49 49 327 108 133 0 638 1 0121 /96 87 47 48 49 332 107 134 0 665 1 0122/96 122 46 50 38 322 106 134 0 692 I 10123/96 86 44 50 39 314 104 134 0 681 1 0124196 96 43 48 41 320 102 133 0 654 1 0125196 107 43 48 38 322 1 01 132 0 701 1 0126196 112 43 48 53 335 1 01 1 32 0 713 I 1 0/27196 117 50 51 63 363 106 141 0 746 1 0/28196 107 35 46 52 320 99 130 0 723 1 Q/29196 11 0 15 47 46 346 1 01 133 0 743 1 0130196 93 1 2 45 41 347 100 135 0 731 I 10/31196 11 8 1 3 46 43 363 101 134 610 735 /.VG: 103 41 50 44 306 112 1 37 154 667 I TOT: 3195 1263 1558 1374 9496 3473 4260 4777 20682 I I I I I I I m OUTERTIER DAILY FLOW: I OCT. 1996: OT-1 OT-2 OT-3 OT-4 OT-5 OT-6 OT-SA OT-7 OT-8 I 1 0/01 /96 20900 9500 1975 1232 3006 6691 5425 2492 17400 1 0/02/96 21000 9500 2001 1246 3045 6475 6215 2608 17800 1 0/03/96 21100 9600 1 971 1243 3009 6304 7233 2586 17600 1 0/04/96 20900 9400 1978 1229 2980 6738 6854 2556 17600 I 10/05/96 20400 9300 1941 1216 2910 6567 5890 2524 17200 1 0/06/96 21300 9700 2026 1265 3014 6845 5926 2554 18000 1 0/07 /96 21100 9600 1961 1224 2909 6616 7076 2476 17600 10/08/96 21400 9800 1999 1251 2944 6641 8156 2592 17800 I 10/09/96 20700 9500 1976 1242 2894 6482 7865 2541 17300 10/10/96 21100 9400 1890 1223 3028 6394 1916 2509 18400 10/11/96 21800 9700 1953 1263 3125 6621 3560 2508 19400 10/12/96 21400 9500 1900 1251 3039 6518 4373 2493 19200 I 10/13/96 20900 9200 1858 1224 2956 6360 3742 2453 18800 1 0/14/96 20400 9100 1805 1205 2889 6271 1562 2401 18400 10/15/96 21200 9400 1831 1247 2986 6430 665 2411 19900 10/16/96 20900 9300 1810 1231 2952 6298 31 2387 19900 I 10/17/96 21300 9500 1853 1239 2965 6240 1 2435 19800 10/18/96 21500 9600 1907 1272 2995 6497 0 2541 19700 10/19/96 21000 9300 1842 1229 2894 6298 0 2424 19100 10/20/96 21000 9300 1835 1243 2900 6261 0 2438 19100 I 10/21 /96 20800 9200 1834 1236 2882 6202 0 2419 19100 1 0/22/96 20700 9200 1845 1235 2878 6219 0 2474 19000 1 0/23/96 20600 9200 1851 1238 2872 6167 0 2468 19100 10/24/96 20700 9100 1847 1235 2871 6243 197 2454 19200 I 1 0/25/96 19600 9000 1825 1220 2845 5950 8703 2402 19100 1 0/26/96 20400 9100 1843 1240 2870 5940 9227 2500 19200 1 0/27 /96 21300 9400 1927 1313 2978 6149 9409 2605 20100 10/28/96 11300 5000 1017 715 1584 3185 5106 1404 10600 I 1 0/29/96 18200 9000 1985 1368 2826 6204 9117 2609 18900 10/30/96 21100 9600 1944 1315 2864 6235 9168 2545 18900 10/31/96 18400 9700 1956 1303 2928 6246 4390 2439 20200 I AVG: 20465 9248 1877 1232 2898 6267 4252 2460 18497 TOT: 634400 286700 58186 38193 89838 194287 131807 76248 573400 I I I I I I I I I GROUNDWATER MONTHLY MONITORING: INNER TIER COMBINED INFLUENT #2 ITCI I PAGENO.1 OCT 1996 DATE: FLOW: PH: COD: TSS: TOG: I GPD pH ppm ppm ppm 10/01 /96 1590 5.7 4490 32 1312 I 1 0/02/96 2023 5.3 6800 1 1 10/03/96 1925 5.6 4650 5 1 0/04/96 1730 5.5 4300 1 9 I 1 0/05/96 1706 5.5 4300 1 0 1 0/06/9.6 1769 5.5 3600 1 3 10/07/96 1924 5.3 5400 1 2 I 1 0/08/96 1963 5.4 5150 15 1490 1 0/09/96 1585 5.6 4900 46 1 0/1 0/96 1534 5.5 4180 1 2 I 10/11/96 1686 5.6 5460 26 1 0/12/96 1423 5.9 5370 21 I 10/13/96 1499 5.5 5660 1 5 10/14/96 1503 5.6 5380 1 1 1 0/15/96 1533 5.5 5490 1 0 1586 I 10/16/96 1510 5.4 4950 1 0 10/17/96 1525 5.6 5930 8 10/18/96 1514 5.4 4780 4 I 1 0/19/96 1451 5.4 4750 8 1 0/20/96 1431 5.4 4850 4 10/21/96 1469 5.5 5380 7 I 1 0/22/96 1510 5.4 5250 4 1719 1 0/23/96 1452 5.4 5410 4 1 0/24/96 1437 5.3 4910 3 I 1 0/25/96 1492 5.4 5430 7 1 0/26/96 1537 5.4 5730 8 10/27/96 1637 5.9 5570 6 I 1 0/28/96 1512 5.4 4920 2 1 0/29/96 1541 5.4 4970 2 1630 1 0/30/96 1504 5.5 5300 5 I 10/31/96 2163 5.6 5420 9 AVG: 1 61 5 5.5 5119 11 1547 I MAX: 2163 5.9 6800 46 1719 MIN: 1423 5.3 3600 2 1312 I I I I I GROUNDWATER MONTHLY MONITORING: OUTER TIER COMBINED INFLUENT: #1 OTCI I PAGENO.1 OCT 1996 DATE: FLOW: PH: TOC: I (?ffi pH ppm 10/01/96 68621 6.7 9 I 1 0/02/96 70090 6.0 1 0/03/96 70646 5.9 1 0/04/96 70235 6.0 I 1 0/05/96 67948 6.0 1 0/06/96 70630 6.0 10/07/96 70562 6.0 I 1 0/08/96 72583 6.1 3 1 0/09/96 70500 6.3 I 10/10/96 65860 5.9 10/11/96 69930 6.0 '1,,- 10/12/96 .69674 6.0 I 10/13/96 67493 5.8 10/14/96 64033 5.9 10/15/96 66070 6.1 · 1 8 I 1 0/16/96 64809 6.3 10/17/96 65333 6.2 1 0/18/96 66012 5.9 I 1 0/19/96 64087 6.2 1 0/20/96 64077 6.1 10/21/96 63673 6.4 I 1 0/22/96 63551 6.0 39 1 0/23/96 63496 5.9 1 0/24/96 63847 5.8 I 1 0/25/96 70645 5.7 1 0/26/96 72320 6.0 10/27/96 75181 5.8 I 1 0/28/96 39911 6. 1 1 0/29/96 70209 6.0 1 5 1 0/30/96 73671 5.9 I 1 0/31 /96 67562 5.8 AVG: 67202 6.0 1 7 I MAX: 75181 6.7 39 MIN: 39911 5.7 3 I I I I I GROUNDWAlER MON1HLY MONITORING: SBR MIXED LIOLOR: SBRML I PAGE N0.4 OCT 1996 SETT. SI.LOGE 5/DAY DATE: PH: NH3N: P04: DO: MLSS: MLVSS: SOLIDS: WASTED FIM: FIM: pH ppm ppm ppm ppm ppm mill gal ratio ratio I 10101196 8.3 101 18.7 1 .8 11 20 90 0 0.41 10102196 8.2 215 22.0 1 .8 1496 1080 95 0 0.29 10103196 8.2 130 15.4 1 .9 1466 100 0 0.28 I 10104196 8.3 159 27.4 1.8 1496 100 0 0.00 10105196 8.3 157 28.0 1.9 1352 100 0 0.29 0.25 10106196 8.2 180 44.0 1 .8 1560 120 ·o 0.24 0.22 10107196 8.3 164 29.8 2.0 1480 11 0 0 0.00 0.16 I 10108196 8.2 171 40.4 2.3 1560 11 5 0 0.28 0.16 10109196 8.2 174 35.6 2. 1 1648 1360 120 . 0 0.24 0.21 10110196 8.2 204 26.0 2.2 1600 120 0 0.00 0.15 10111196 8. 1 168 33.6 2. 1 2148 125 0 0.18 0.14 I 10112196 8.0 172 34.0 2.2 2080 130 0 0.00 0.14 10113196 8.2 164 30.0 2.0 2000 90 0 0.00 0.08 10114196 8.1 196 31.8 2.0 2724 130 0 0.00 0.04 I 1 011 5196 8.2 166 28.1 1.9 2220 145 0 0.20 0.07 10116196 8. 1 158 28.8 2. 1 1920 1408 140 0 0.00 0.04 10117196 8.2 197 17.6 2.2 2978 150 0 0.15 0.07 10118196 8. 1 154 18.8 2.8 1956 155 0 0.00 0.07 I 10119196 8.2 152 20.0 2.0 1984 150 0 0.19 0. 11 1 0120196 8. 1 189 30.0 1.9 2260 160 0 0.17 0.10 10121196 8.2 249 38.0 2.2 2576 170. 0 0.00 0.10 10122196 8.2 227 45.2 2.1 3140 160 0 0.12 0.10 I 10123196 8. 1 208 24.2 2.0 2788 2268 170 0 0.00 0.10 10124196 8.0 210 30.0 2.2 2600 170 0 0.16 0.09 1 0125196 8.1 200 32.0 2. 1 2864 180 0 0.00 0.06 10126196 8. 1 190 30.0 2.2 2484 180 0 0.19 0.09 I 1 0127196 8.0 164 28.0 1 .9 1324 190 0 0.34 0.14 10128196 8. 1 135 21.2 2.1 2276 200 0 0.00 0.14 1 0129196 8.2 218 27.2 2.1 2892 200 0 0.13 0.13 10130196 8.1 152 22.6 1.9 2748 1936 200 0 0.00 0.13 I 10131196 8.0 186 32.6 2.0 2440 210 0 0.21 0.14 AVG: 8.2 178 29 2 2103 1610 144 0 0.13 0.12 I MAX: 8.3 249 45 3 3140 2268 210 0 0.41 0.25 MIN: 8.0 101 1 5 2 1120 1080 90 0 0.00 0.04 I I I I I I I I GROUNDWATER MONTHLY MONITORING: AFTER PLATE SEPARATOR BEFORE SBR: SBRI I PAGENO.3 OCT 1996 DATE: PH: COD: TSS: I pH ppm ppm 10/01 /96 5.6 5140 68 I 1 0/02/96 5.7 4900 20 1 0/03/96 5.9 4550 56 1 0/04/96 I 1 0/05/96 6.9 4400 20 1 0/06/96 6.0 4200 24 10/07/96 I 1 0/08/96 6.3 4950 32 10/09/96 6.2 4380 20 10/10/96 I 10/11/96 5.9 4250 11 2 10/12/96 10/13/96 I 10/14/96 10/15/96 6.0 4970 40 I 10/16/96 10/17/96 5.9 5080 48 1 0/18/96 I 1 0/19/96 6.0 4300 32 1 0/20/96 6.5 4400 24 10/21 /96 I 1 0/22/96 6.2 4400 1 2 1 0/23/96 1 0/24/96 6.0 4570 28 I 1 0/25/96 1 0/26/96 6.6 5210 40 10/27/96 6.4 5110 56 I 1 0/28/96 1 0/29/96 5.6 4280 40 1 0/30/96 I 10/31/96 5.7 5760 44 AVG: 6.1 4714 40 I MAX: 6.9 5760 11 2 MIN: 5.6 4200 1 2 I I I I I GROUNDWATER MONTHLY MONrrORING: I SBR EFFLUENT:(DECANT) #4SBRE PAGENO.5 OCT 1996 WAS. NH3N PHOS. I DATE: FLOW: COD: TSS: TSS ADDED: ADDED: GPO ppm ppm ppm gal lbs I 10/01/96 2265 1 91 82 2 10/02/96 2415 210 120 0 1 0/03/96 2340 190 88 2 1 I 1 0/04/96 0 160 56 1 0 1 0/05/96 2103 190 92 1 0 1 0/06/96 2446 180 80 1 1 I 10/07/96 0 180 60 1 1 1 0/08/96 2347 195 80 0 0 1 0/09/96 2433 185 48 0 0 1· 1 0/1 0/96 0 192 88 0 0 10/11/96 2441 196 80 0 0 1 0/12/96 2534 203 100 1 1 I 10/13/96 0 1 1 10/14/96 0 200 56 0 0 10/15/96 2462 198 42 0 0 I 1 0/16/96 0 205 104 1 1 10/17/96 2538 234 128 0 0 10/18/96 0 210 20 1 1 I 1 0/19/96 2495 205 80 1 1 10/20/96 2450 200 56 1 1 10/21/96 0 210 80 0 0 I 1 0/22/96 2255 235 48 0 0 1 0/23/96 0 250 56 0 0 10/24/96 2488 220 64 0 0 I 1 0/25/96 0 229 56 0 0 10/26/96 2513 260 72 1 1 10/27/96 2527 213 80 1 1 I 1 0/28/96 ·O 205 64 1 1 1 0/29/96 2113 198 80 0 0 1 0/30/96 0 205 84 1 1 I 1 0/31 /96 2532 261 44 1 1 AVG: 1474 207 73 0 1 1 I MAX: 2538 261 128 0 2 1 MIN: 0 160 20 0 0 0 I I I I m GROUNDWATER MONTHLY MONITORING: INNER TIER EQUALIZATION TANK: ITEQT u PAGENO.2 OCT 1996 DATE: PH: COD: OT WATER ADDED I pH ppm gal 10/01/96 7.3 5080 I 1 0/02/96 7.4 4850 1 0/03/96 7.2 4200 1 0/04/96 7.4 4350 I 1 0/05/96 7.5 4400 185.0 1 0/06/96 7.2 3950 10/07/96 7.2 4600 I 10/08/96 7.2 4800 10/09/96 7.4 3900 340.0 I 1 0/1 0/96 7.3 4500 10/11/96 7.2 4180 10/12/96 7.1 5240 I 10/13/96 7.2 5190 1 0/14/96 7 .1 4900 10/15/96 7.4 4890 I 1 0/16/96 7.5 4700 10/17/96 7.4 5030 1 0/18/96 7.9 4060 I 10/19/96 7.6 4250 1 0/20/96 7.5 4550 375 1 0/21 /96 7.9 4600 I 1 0/22/96 7.7 4650 1 0/23/96 7.6 4770 1 0/24/96 7.7 4710 I 1 0/25/96 8.2 5160 1 0/26/96 7.4 5020 10/27/96 7.7 5040 375 I 1 0/28/96 7.7 4340 1 0/29/96 7.6 4340 10/30/96 7.5 5000 I 10/31 /96 7.4 5610 AVG: 7.5 4673 319 I MAX: 8.2 5610 375 MIN: 7.1 3900 185 I I I m I GROUNDWATER MONTHLY MONITORING: INNER TIER CARBON FILTER EFFWENT #8 ITEF I PAGE NO. 7 OCT 1996 DATE: PH: COD: TOC: TSS: I pH ppm ppm ppm 10/01/96 1 03 I 1 0/02/96 8.3 190 28 1 0/03/96 1 0/04/96 I 1 0/05/96 1 0/06/96 10/07/96 I 1 0/08/96 37 1 0/09/96 8.1 165 I 1 0/1 0/96 10/11/96 1 0/12/96 I 10/13/96 10/14/96 10/15/96 49 I 10/16/96 10/17/96 8.3 211 10/18/96 I 1 0/19/96 1 0/20/96 10/21/96 I . 1 0/22/96 227 1 0/23/96 1 0/24/96 8.2 203 I 1 0/25/96 1 0/26/96 10/27/96 I 1 0/28/96 1 0/29/96 56 1 0/30/96 I 10/31/96 8.4 252 AVG: 8.3 204 94 28 I MAX: 8.4 252 227 28 MIN: 8. 1 165 37 28 I I I I I GROUNDWATER MONTHLY MONITORING: I OUTER TIER CARBON FILTER EFFLUENT: #7 OTEF PAGENO.3 OCT 1996 I DATE: PH: TOC: TSS: pH ppm ppm g 10/01/96 8 1 0/02/96 6.9 3 1 0/03/96 I 1 0/04/96 1 0/05/96 10/06/96 I 10/07/96 1 0/08/96 3 1 0/09/96 6.8 I 1 0/1 0/96 10/11/96 10/12/96 I 1 0/13/96 10/14/96 10/15/96 6 I 10/16/96 6.9 10/17/96 1 0/18/96 I 10/19/96 1 0/20/96 10/21/96 •· 1 0/22/96 7 1 0/23/96 1 0/24/96 7.8 I 1 0/25/96 1 0/26/96 10/27/96 I 1 0/28/96 1 0/29/96 6 1 0/30/96 I 10/31/96 5.8 AVG: 6.8 6 3 I . MAX: 7.8 8 3 MIN: 5.8 3 3 I I I I I GROUNDWATER MONTHLY MONITOF I RAINFALL DATA I DATE INCHES/DAY I 10/01/96 0.00 1 0/02/96 0.00 1 0/03/96 0.00 I 1 0/04/96 0.00 1 0/05/96 0.00 1 0/06/96 0.00 I 10/07/96 1.20 1 0/08/96 0.00 1 0/09/96 0.00 I 10/10/96 0.00 10/11/96 0.00 1 0/12/96 0.00 I 10/13/96 0.00 10/14/96 0.00 10/15/96 0.00 I 1 0/16/96 0.00 10/17/96 0.00 1 0/18/96 0.00 I 1 0/19/96 0.00 1 0/20/96 0.00 10/21/96 0.00 I I 0/22/96 0.00 1 0/23/96 0.00 1 0/24/96 0.00 I 1 0/25/96 0.00 10/26/96 0.00 10/27/96 0.00 I 1 0/28/96 0.00 1 0/29/96 0.00 1 0/30/96 0.00 I 10/31/96 0.00 I TOTAL 1.20 I I I g I I I I I I I I I I I I I I I I I I MAINTENANCE ACTIVrTIES-OROUNDWATER OPERABLE UNIT #1 NNER TIER SYSTEM DATE LOCATION 1 0/05/96 IT-5 1 0/07 /96 IT-8 PRC8.EM LOW FLOW LOW FLOW ACTION DATE 10/05/96 10/31/96 ACTION REPLACED 81.AODER REPLACED PUMP.REPLACED WATER LINES TO PUMP PPJP JPPP I I I I I I I I I I I I I I I I I I MAINTENANCE ACTIVITIES-OROUNDWATER OPERABLE UNIT #1 OUTER llER SYSTEM DATE LOCATION 1 0/08/96 OT-6A PR:aEM NO FLOW ACllON DATE 10/25/96 ACllON REPLACED FLOW METER SET FLOW RATE MECHPNIC PPJP I I INNER TIER DAILY FLOW: I NOV. I 1996: IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9 11/01/96 1 13 1 4 48 40 361 1 02 135 1018 7 57 11 /02/96 86 1 5 44 40 305 98 123 0 724 I 11 /03/96 82 17 46 44 202 99 139 0 733 11 /04/96 68 14 46 48 344 98 132 618 481 11 /05/96 99 20 45 43 339 95 130 691 727 11 /06/96 11 6 5 45 59 336 90 134 980 727 I 11/07/96 89 12 1 3 58 267 79 107 545 589 11 /08/96 88 19 1 9 100 387 87 119 2944 390 11 /09/96 98 18 4 81 189 100 142 5129 739 11/10/96 99 1 8 2 78 175 99 132 4276 726 I 11/11/96 77 1 8 1 8 77 1 81 99 132 791 727 11/12/96 98 1 5 29 69 199 82 104 631 640 11/13/96 91 13 39 72 318 93 119 698 6 11/14/96 120 22 34 79 335 101 133 733 67 I 11/15/96 113 18 36 84 183 103 127 758 0 11/16/96 164 17 34 81 342 100 122 728 0 :1/17/96 130 1 8 34 81 334 99 120 732 0 11/18/96 121 1 7 34 81 319 98 120 729 0 I 11/19/96 1 1 8 1 8 26 80 314 99 120 717 30 11 /20/96 113 1 7 22 78 304 99 11 8 719 400 11/21/96 1 1 5 1 8 21 78 302 96 118 709 269 11 /22/96 116 1 8 21 79 307 99 121 725 332 I 11/23/96 130 1 8 21 79 322 98 1 21 723 394 11 /24/96 106 1 6 19 74 311 92 111 675 436 11 /25/96 89 1 7 22 70 277 88 108 680 435 11 /26/96 111 1 7 20 77 217 97 123 714 399 I 11/27/96 111 17 20 77 347 96 119 729 359 11/28/96 104 17 20 71 314 90 112 688 331 11 /29/96 124 1 8 21 79 361 100 132 759 434 11 /30/96 1 06 1 5 19 81 291 84 108 631 480 I ft'✓G: 1 07 17 27 71 293 95 123 1016 411 I TOT: 3195 496 822 2138 8783 2860 3681 30470 12332 I I I I I I I I OUTER TIER DAILY FLOW: I NOV. 1996: OT-1 OT-2 OT-3 OT-4 OT-5 OT-6 OT-SA OT-7 OT-8 11/01/96 21300 9600 1931 1288 2874 5963 4028 2421 20000 I 11 /02/96 21400 9700 1938 1287 2874 6145 4193 2417 20000 11 /03/96 20800 9400 1887 1262 2789 5996 4106 2349 19800 11 /04/96 20900 9500 1930 1284 2792 6003 4519 2403 20100 11 /05/96 20400 9300 1892 1291 2708 5927 9144 2482 19000 I 11 /06/96 20400 9200 1893 1309 2663 5712 9477 2499 18700 11 /07/96 21700 9800 2052 1427 2769 6019 9823 2659 19700 11 /08/96 17300 8100 1782 1223 2176 5366 7736 2275 15900 I 11/09/96 15100 8100 1910 1346 1814 5299 6239 2483 13400 11/10/96 22800 10400 1851 1318 2550 5949 7852 2344 19700 11/11/96 22800 10600 1939 1331 2543 5847 8248 2342 19600 11/12/96 22600 10500 1841 1356 2497 5868 0 2381 19600 11/13/96 22600 10500 1903 1392 2460 5884 7768 2389 19800 I 11/14/96 22100 10000 1988 1382 2361 5769 8765 2398 19200 11/15/96 20700 8800 2010 1394 2201 5997 8232 2363 18100 11/16/96 9400 8900 2059 1331 1705 6371 6166 2427 13500 I 11/17/96 26900 11600 1932 1342 2291 5858 8630 2452 19900 11/18/96 21600 12100 2052 1365 2250 5890 8703 2429 19600 11/19/96 21700 10900 1966 1391 2187 5978 8572 2396 19400 11/20/96 21600 10800 2043 1413 2159 5891 8074 2379 19400 I 11/21/96 21600 10600 2034 1450 2141 5699 7784 2340 19300 11 /22/96 21700 10600 2013 1486 2122 5742 7997 2360 19200 11/23/96 22300 10900 2087 1545 2155 5975 8357 2426 19800 11/24/96 21200 10300 1988 1512 2028 5657 7876 2355 18700 I 11 /25/96 21700 10600 2049 1 567 2053 5721 7970 2472 19100 11 /26/96 21400 10400 2014 1544 2015 5599 7874 2337 18900 11/27/96 21400 10400 1980 1337 2012 5610 7710 2331 18900 11 /28/96 21700 10500 2039 1 361 2019 5710 7943 2365 19200 I 11 /29/96 21700 10500 2046 1391 1992 5751 7861 2378 19200 11 /30/96 21500 10400 2035 1410 1945 5648 7882 2381 19100 I AVG: 21010 10100 1969 1378 2305 5828 7318 2401 18860 TOT: 630300 303000 59084 41335 69145 174844 219529 72033 565800 I I I I I I I I • GROUNDWATER MONTHLY MONITORING: INNER TIER COMBINED INFLUENT #2 ITCI I PAGENO.1 NOV.1996 DATE: FLOW: PH: COD: TSS: TOC: m (?ffi pH ppm ppm ppm 11/01/96 2588 5.5 4800 71 m 11/02/96 1435 5.4 4960 1 4 11/03/96 1362 5.3 4510 1 2 11/04/96 1849 5.3 4870 1 0 m 11/05/96 2189 5.5 5620 3 1540 11/06/96 2192 5.4 4930 9 11/07/96 1759 5.4 5030 1 0 g 11/08/96 4053 5.7 5130 9 11/09/96 6500 5.8 5240 1 0 11/10/96 5605 5.7 5410 9 0 11/11/96 2120 5.4 4740 9 11/12/96 1867 5.5 4840 8 1440 11 / 13/96 1449 5.4 5190 1 2 0 11/14/96 1624 5.4 5160 1 0 11/15/96 1422 5.4 7120 7 11/16/96 1558 5.4 8400 9 D 11/17/96 1548 5.4 6980 5 11/18/96 1519 5.5 7610 8 11/19/96 1522 5.1 7530 14 2155 0 11/20/96 1870 5.4 7270 6 11/21/96 1726 5.4 6170 4 11/22/96 1818 5.3 4730 4 o· 11 /23/96 1906 5.6 4950 1 4 11/24/96 1840 5.7 6000 1 1 11/25/96 1786 5.4 4300 5 D 11 /26/96 1875 5.4 4930 3 1581 11/27/96 1875 5.4 7100 11 11/28/96 1747 5.4 3980 1 0 D 11/29/96 2028 5.4 4810 3 11 /30/96 1815 5.8 3140 7 fl AVG: 2148 5.5 5515 1 1 1679 I MAX: 6500 5.8 8400 71 2155 · MIN: 1362 5.1 3140 3 1440 • m I I I GROUNDWATER MONTHLY MONITORING: OUTER TIER COMBINED INFLUENT: #1 OTCI m PAGENO.1 NOV.1996 DATE: FLOW: PH: TOC: m GPD pH ppm 11/01/96 69405 6.5 m 11/02/96 69954 6.4 11 /03/96 68389 6.0 11 /04/96 69431 5.9 m 11/05/96 72144 5.8 7 11/06/96 71853 5.9 11/07/96 75949 5.9 m 11/08/96 61758 5.9 11/09/96 55691 5.8 11/10/96 74764 5.8 -11/11/96 75250 6.8 11/12/96 66633 6. 1 3 11/13/96 74696 5.8 I 11/14/96 73963 6.0 11/15/96 69797 6.0 11/16/96 50589 5.9 I 11/17/96 80905 5.9 11/18/96 75989 5.8 11/19/96 74490 5.9 3 I 11/20/96 73759 6.0 11/21/96 72948 6.0 11/22/96 73221 5.9 I 11 /23/96 75545 6.0 11/24/96 71626 6.3 I 11/25/96 73232 6.0 11/26/96 72083 6.0 6 11/27/96 71680 6.0 I 11/28/96 72837 6.1 11/29/96 72819 5.9 11/30/96 72301 6.0 I AVG: 71123 6.0 5 I MAX: 80905 6.8 7 MIN: 50589 5.8 3 I I I I m GAOUNDWA1ER IJONTHLY MONITORING: SBA MIXED LIQUOR: S8RML PAGE N0.4 g NOV.1996 SETT. SlLOOE 5/DAY DATE: PH: NH3N: P04: DO: MLSS: MLVSS: SOLIDS: WAS1ED F/M: F/M: pH ppm ppm ppm ppm ppm ml/I gal ratio ratio I 11/01/96 8.3 163 32.0 2.0 1764 235 0 0.23 11 /02/96 8.2 168 30.6 1.9 1900 250 0 0.00 11 /03/96 8.3 187 24.8 3.0 1920 240 0 0.24 I 11 /04/96 8.2 179 18.0 2.5 1972 275 0 0.00 11 /05/96 8.1 217 35.2 2.2 2804 280 0 0.18 0.13 11/06/96 8.2 184 29.4 2.7 2240 285 0 0.16 0.12 11/07/96 8.2 176 17.6 3.5 2664 310 0 0.00 0.12 I 11/08/96 8.1 222 36.8 2.9 2580 390 0 0.15 0.10 11 /09/96 8.2 220 38.0 3.0 2400 395 0 0.16 0.13 11/10/96 8.1 200 36.0 2.4 2176 530 0 0.00 0.09 11/11/96 7.7 161 17.2 3.3 2000 400 0 0.19 0.10 I 11/12/96 7.6 152 18.8 2.9 3360 510 0 0.00 0.10 11/13/96 7.5 170 24.0 3.0 3824 520 150 0.08 0.09 11/14/96 8.2 150 22.0 2.9 3600 800 135 0.08 0.07 11/15/96 8.2 152 21.0 2.8 2456 850 121 0.17 0.10 I 11/16/96 8.2 190 20.0 2.7 2500 1000 121 0.00 0.07 11/17/96 8.2 199 53.0 2.7 2656 950 25 0.00 0.07 11/18/96 8.1 191 38.4 2.9 2724 975 121 0.22 0.10 I 11/19/96 8.2 145 32.8 2.6 3756 975 135 0.00 0.08 11/20/96 8.2 196 28.9 2.6 2940 1000 135 0.17 0.08 11/21/96 8.2 168 23.6 2.4 2992 1000 175 0.00 0.08 11 /22/96 8.1 228 30.4 2.7 2732 1000 275 0.16 0.11 I 11 /23/96 8.3 206 28.0 3.1 2488 1000 135 0.19 0.10 11 /24/96 8.2 182 32.0 3.2 2692 1000 121 0.00 0.10 11 /25/96 8.2 156 16.8 3.1 2760 975 269 0.14 0.10 11 /26/96 8.2 132 12.8 3.1 2712 990 202 0.17 0.13 I 11/27/96 8.2 132 27.2 3.0 2864 1000 121 0.00 0.10 11 /28/96 8.2 175 34.8 3.1 2576 990 130 0.15 0.09 11 /29/96 8.2 118 23.2 3.0 2612 990 202 0.19 0.13 11/30/96 8.2 137 9.8 2.9 2292 980 0 0.00 0.10 I AVG: 8.1 175 27 3 2632 0 703 86 0.10 0.10 MAX: 8.3 228 53 4 3824 0 1000 275 0.24 0.13 I MIN: 7.5 118 1 0 2 1764 0 235 0 0.00 0.07 I I I I I I I m GROUNDWATER MONTHLY MONITORING: AFTER PLATE SEPARATOR BEFORE SBR: SBRI I PAGENO.3 NOV.1996 DATE: PH: COD: TSS: D pH ppm ppm 11/01/96 5.7 4600 24 I 11/02/96 11/03/96 6.3 5290 1 6 11/04/96 I 11/05/96 6.0 5530 84 11/06/96 5.5 3990 24 11/07/96 I 11/08/96 5.6 4450 40 11/09/96 5.8 4410 44 11/10/96 I 11/11/96 5.8 4220 40 11/12/96 I 11/13/96 5.0 3360 20 11/14/96 5.9 3390 36 11/15/96 6.0 4780 20 I 11/16/96 11/17/96 11/18/96 6.0 6750 40 I 11/19/96 11 /20/96 5.9 5710 44 11/21/96 I 11/22/96 6.0 4810 40 11/23/96 6.8 5370 24 11/24/96 I 11/25/96 6.0 4300 24 11/26/96 6.0 5060 8 11/27/96 I 11/28/96 6.1 4230 24 11/29/96 6.6 5540 4 11/30/96 I AVG: 5.9 4766 31 I MAX: 6.8 6750 84 MIN: 5.0 3360 4 I I I I I GROUNDWATER MONTHLY MONITORING: SBR EFFLUENT:(DECANT) #4SBRE I PAGENO.5 NOV.1996 WAS. NH3N PHOS. DATE: FLOW: COD: TSS: TSS ADDED: ADDED: 0 (:fl) ppm ppm ppm gal lbs 11/01/96 2385 215 104 1 I 11/02/96 0 230 76 0 11 /03/96 2267 260 92 1 11/04/96 0 235 100 1 1 I 11 /05/96 2452 309 112 0 0 11/06/96 2494 162 104 0 0 11/07/96 0 215 80 1 1 I 11/08/96 2370 201 136 0 0 11/09/96 2576 2·1 0 160 1 1 11/10/96 0 1 81 176 0 0 I 11/11/96 2398 160 11 6 1 1 11/12/96 0 155 44 1 1 11/13/96 2400 179 64 1 1 I 11/14/96 2489 182 80 5060 1 1 11/15/96 265 100 1 1 11/16/96 1778 260 84 4160 1 1 I 11/17/96 0 190 100 5280 0 0 11/18/96 2214 200 108 5400 1 0 I 1 1 / 1 9 /9 6 0 199 48 4400 1 1 11/20/96 2202 821 160 10820 1 1 11/21/96 0 174 68 4900 1 1 I ·11/22/96 1902 200 120 6040 0 0 11/23/96 2252 230 120 4660 0 0 11/24/96 0 190 92 5200 0 0 I 11/25/96 1884 795 570 4720 1 1 11/26/96 2276 515 156 3540 1 2 11/27/96 0 201 80 4560 1 1 I 11/28/96 1630 190 76 3980 0 0 11/29/96 2147 162 44 3080 1 11/30/96 0 240 72 1 1 I AVG: 1337 258 115 5053 1 1 I MAX: 2576 821 570 10820 1 2 MIN: 0 155 44 3080 0 0 I I I I I GROUNDWATER MONTHLY MONITORING: INNER TIER EQUALIZATION TANK: ITEQT I PAGENO.2 NOV.1996 DATE: PH: COD: OT WATER ADDED I pH ppm gal 11/01/96 7.4 4700 I 11/02/96 7.4 4800 11/03/96 7.2 4800 11/04/96 7.2 4480 I 11/05/96 7.2 5850 11/06/96 7.3 4630 11/07/96 7.3 5480 I 11/08/96 7.4 4680 11/09/96 7.3 4540 11/10/96 7.2 5350 I 11/11/96 7.3 4180 11/12/96 7.4 4220 11/13/96 7.3 3710 I 11/14/96 7.2 3680 11/15/96 7.2 · 5250 I 11/16/96 7.2 5800 11/17/96 7.2 6300 11/18/96 7.1 6800 I 11/19/96 7.2 7230 11/20/96 7.2 6510 11/21/96 7.2 5170 I 11/22/96 7.3 5570 11/23/96 7.5 5420 11/24/96 7.5 5100 I 11/25/96 7.2 4500 11/26/96 7.2 4820 400 11/27/96 7.3 4950 I 11/28/96 7.2 4520 11/29/96 7.3 4800 11/30/96 7.5 2990 I AVG: 7.3 5028 400 I MAX: 7.5 7230 400 · MIN: 7.1 2990 400 I I I g I GROUNDWATER MONTHLY MONITORING: INNER TIER CARBON FILTER EFFWENT #8 ITEF I PAGE NO. 7 NOV.1996 DATE: PH: COD: TOC: TSS: I pH ppm ppm ppm 11/01/96 I 11/02/96 11/03/96 11/04/96 I 11/05/96 37 11/06/96 8.3 168 36 11/07/96 I 11/08/96 11/09/96 11/10/96 I 11/11/96 11/12/96 1 8 1 1 / 13/96 8.3 189 I 11/14/96 11/15/96 I 11/16/96 11/17/96 11/18/96 I 11/19/96 59 11/20/96 8.0 310 11 /21 /9 6 I 11/22/96 11 /23/96 11/24/96 I 11 /25/96 11/26/96 64 11/27/96 I 11/28/96 8.3 311 11/29/96 11/30/96 I AVG: 8.2 245 45 36 I MAX: 8.3 311 64 36 MIN: 8.0 168 1 8 36 I I I I I GROUNDWATER MONTHLY MONITORING: OUTER TIER CARBON FILTER EFFLUENT: #7 OTEF I PAGENO.3 NOV.1996 DATE: PH: TOC: TSS: I pH ppm ppm I 11/01/96 11/02/96 11/03/96 I 11/04/96 11/05/96 3 11/06/96 6.8 4 I 11/07/96 11 /08/96 11/09/96 I 11/10/96 11/11/96 11/12/96 4 I 11/13/96 6.9 11/14/96 11/15/96 I 11/16/96 11/17/96 11/18/96 I 11/19/96 8 11/20/96 6.8 11/21/96 I 11 /22/96 11/23/96 11/24/96 I 11/25/96 11/26/96 4 11/27/96 I 11 /28/96 7.0 11 /29/96 11/30/96 I AVG: 6.9 5 4 I MAX: 7.0 8 4 MIN: 6.8 3 4 I I I I D GROUNDWATER MONTHLY MONITOF I RAINFALL DATA I DATE INCHES/DAY I 11/01/96 0.70 11/02/96 0.00 11/03/96 0.00 I 11/04/96 0.00 11 /05/96 0.10 11/06/96 0.00 I 11/07/96 1.00 11/08/96 . 1.50 11/09/96 0.00 I 11/10/96 0.00 11/11/96 0.00 11/12/96 0.00 I 11/13/96 0.00 11/14/96 0.00 11/15/96 0.00 I 11/16/96 0.00 11/17/96 0.00 11/18/96 0.80 I 1 1 / 1 9 /9 6 0.00 11/20/96 0.00 11/21/96 0.60 I 11/22/96 0.00 11/23/96 0.00 11/24/96 0.00 I 11/25/96 0.50 11/26/96 0.00 11/27/96 0.00 I 11 /28/96 0.00 11/29/96 0.20 11/30/96 1.90 I TOTAL 7.30 I I I I I g I I I I I I I I I I I I I I I I I MAJmENANCE ACTIVITIES{;ROUNDWATER OPERABLE UNIT #1 NNER TIER SYSTEM DATE LOCATION Pf03.EM 11 /04/96 IT-8 LOWR.OW 09/16/96 IT-2 LOWR.OW 09/09/96 rr-1 LOWR.OW 10/07/96 IT-4 LOWR.OW 11/11/96 IT-1 LOWR.OW 11/11/96 IT-2 LOWR.OW 11/11/96 IT-8 LOWR.OW 11/10/96 IT-3 LOWR.OW 11/17/96 IT-9 NOA.OW 11/21/96 rr-e NOA.OW ACTICN DATE ACTICN MECHANIC 11 /04/98 REPI.ACED PUMP,ClEANED STRAINER UNP\.UGED LINE JPPP 11/05/98 REPI.ACED Bl.ADDER ClEANED STRAINER JPPP 11/05/96 REPI.ACED Bl.ADDER JPPP 11/06/96 REPI.ACED WATER LINES IN WELL JPPP 11/11/96 REP\.ACED A.OW METER& PIPING JPPP TO HEADER PIPE. 11/11/96 REP\.ACED Bl.ADDER,ClEANED SCREEN JPPP 11/11/96 ADJUSTED R.OAT IN PUMP JPPP 11/19/96 ADDED 6 GAL. WATER TO WELL PPLB REP\.ACED TUBING.SET PUMP TO ORGINAI. DEPTH 11 /20/96 REP\.ACED PROB, WIRES PPRR 11/21/96 RESET PUMP &SET A.OW RATE pp I g I I I I I I I I I I I I I I I I MAINTENANCE ACT!VrTIES<3ROUNDWATER OPERABLE UNIT #1 OUTER TIER SYSTEM DATE LOCATION PACae,1 11 /04/96 OT-6A LOW FLOW 1 0/09/96 OT-2 LOW FLOW 11/13/96 OT-6A NO FLOW 11/22/96 OT-6 LEAK ACTION DATE 11 /05/96 11/05/96 11/14/96 11 /22/96 ACTION SET FLOW TO 7.5 GPM REPLACED Bu\DDER CLEANED SCREEN REPLACED FLOW METER REPLACED FLOW SWITCH MECHANIC PPJP JPPP PPJP RAPP I m INNER11ER DAILY FLOW: g_ [EC I 1996: IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9 12/01 /96 100 1 7 220 189 261 86 107 675 485 12/02/96 1 09 17 44 79 314 98 129 716 550 I 12/03/96 1 1 0 16 27 72 247 · 1 01 118 713 409 12/04/96 1 09 17 25 75 252 103 1 21 719 508 12/05/96 98 16 58 68 262 93 11 8 672 467 12/06/96 104 16 55 74 320 104 134 741 454 I 12/07/96 96 1 5 145 67 279 96 112 651 369 1 2/08/96 92 1 8 49 68 217 96 11 0 644 444 1 2/09/96 97 26 1 7 76 1 51 103 136 724 247 12/10/96 1 51 20 56 76 340 105 11 0 845 31 I 12/11/96 1 42 1 8 27 69 355 111 1 11 111 542 12/12/96 1 11 f5 558 57 282 91 11 7 0 434 12/13/96 1 31 21 83 73 257 1 08 133 1 563 12/14/96 136 18 31 83 319 112 1 50 0 458 I 12/15/96 142 20 27 80 302 120 158 0 467 12/16/96 139 19 27 77 384 123 160 738 472 12/17/96 140 20 56 80 341 122 139 890 437 12/18/96 1 51 20 1 41 97 372 122 138 888 548 I 12/19/96 1 06 23 108 106 143 122 . 138 904 105 12/20/96 1 01 1 9 37 99 129 125 137 955 0 \ 2/21 /96 1 05 20 25 1 01 1 21 114 136 635 0 '2/22/96 1 51 21 28 11 5 283 127 178 0 0 I 12/23/96 156 21 28 11 0 404 127 1 81 1020 0 1 2/24/96 142 21 31 114 303 128 177 1094 0 12/25/96 136 21 28 118 182 130 173 1117 0 12/26/96 11 0 1 4 1 9 83 249 91 11 0 796 332 I 1 2/27 /96 98 1 7 23 74 220 81 95 753 392 1 2/28/96 1 39 24 30 105 335 121 162 1134 583 1 2/29/96 137 21 38 113 302 123 172 1127 584 12/30/96 150 22 34 124 210 139 188 1261 644 I 12/31/96 149 22 389 122 11 0 137 189 1381 645 AVG: 124 1 9 79 92 266 112 140 707 360 I TOT: 3838 595 2464 2844 8246 3459 4337. 21905 11170 I I I I I I D g OUTER TIER DAILY FLOW: I DEC. 1996: OT-1 OT-2 OT-3 OT-4 OT-5 OT-6 OT-6A OT-7 OT-8 I 12/01 /96 21500 10300 2032 1442 1893 5749 7770 2419 18800 12/02/96 21500 10400 2025 1445 1861 5867 7854 2326 19000 12/03/96 21500 10300 2009 1468 1836 5848 7683 2345 18900 1 2/04/96 21500 10400 2034 1490 1806 5976 7913 2356 19100 I 12/05/96 21300 10300 2036 1485 1761 5964 7912 2334 19000 12/06/96 21200 10200 2017 1464 1828 5837 7716 2325 18600 1 2/07 /96 21900 10500 2079 1 523 1850 6000 8035 2413 19400 1 2/08/96 21300 10200 2030 1495 1769 5819 7782 2332 19000 I 12/09/96 21200 1 0200 2022 1514 1751 5795 7702 2305 19600 12/10/96 21500 1 0300 2049 1524 1751 5850 7841 2346 19800 12/11/96 20900 10100 2053 1 511 1697 5818 7808 2431 19400 12/12/96 20900 10100 1865 1279 1814 5725 7390 2350 19500 I 12/13/96 22100 10700 1840 1342 1862 5907 7960 2407 20700 12/14/96 21000 10100 1741 1306 1726 5753 7513 2281 19700 12/15/96 21400 10300 1791 1369 1741 5889 7624 2370 20200 12/16/96 21500 10300 1813 1396 1705 5913 7599 2345 20000 I 12/17/96 19600 9700 1846 1358 1573 5885 7478 2345 18500 12/18/96 15100 7900 2029 1299 1262 5124 5986 2417 14700 12/19/96 21100 10200 2053 1320 1677 6027 7416 2315 20600 12/20/96 22000 10600 2122 1353 1741 6077 8169 2362 21400, I 12/21/96 22200 10600 2179 1412 1771 6103 8390 2432 21400 1 2/22/96 20800 10100 2059 1357 1675 5786 7715 2341 20200 12/23/96 22600 10600 1963 1428 1786 5879 4020 2313 24900 12/24/96 17600 8600 1853 11 51 1418 4926 6190 1888 1 8000 I 12/25/96 21800 10500 2129 1351 1 711 6221 7568 2317 22900 1 2/26/96 21500 10400 2160 1383 1658 6162 7584 2319 22000 1 2/27 /96 21400 10400 2167 1412 1629 6092 7511 2323 22000 12/28/96 21300 10300 2155 1434 1597 6048 7853 2299 21500 I 12/29/96 21200 10300 2147 1451 1571 6078 8001 2302 21400 12/30/96 21300 10300 2141 1443 1570 5944 7864 2298 21200 12/31/96 21700 10500 2175 1487 1590 6028 7490 2344 21600 I AVG: 21077 10184 2020 1409 1706 5874 7527 2332 20097 TOT: 653400 315700 62614 43692 52880 182090 233337 72300 623000 I I I I I I I I I GROUNDWATER MONTHLY MONrrORING: INNER TIER COMBINED INFLUENT #2 ITCI I PAGENO.1 DEC 1996 DATE: FLOW: PH: COD: TSS: TOC: I GD pH . ppm ppm ppm 12/01/96 2140 5.7 4850 4 I 12/02/96 2056 5.8 4850 1 1 12/03/96 1813 5.5 4900 1 0 1170 1 2/04/96 1929 5.4 7918 9 I 12/05/96 1852 5.5 6560 1 0 12/06/96 2002 5.8 4030 5 12/07/96 1830 5.9 5510 6 'I 12/08/96 1738 5.8 4220 12 12/09/96 1577 5.5 3750 6 1248 I 12/1 0/96 1734 5.6 6000 9 12/11/96 1486 5.6 8030 31 12/12/96 1665 5.6 5860 30 I 12/13/96 1370 5.5 7270 1 8 12/14/96 1307 5.4 4850 1 2 12/15/96 1316 5.3 5420 1 1 I 12/16/96 2139 5.6 4270 1 1 12/17/96 2225 5.8 4190 1 0 1874 12/18/96 2477 5.7 6910 15 I 12/19/96 1755 5.7 4480 9 12/20/96 1602 5.6 6320 9 12/21/96 1257 5.8 6930 8 I 12/22/96 903 5.9 7210 6 1 2/23/96 2047 5.4 8660 1 0 1 2/24/96 2010 5.6 5120 9 1584 I 12/25/96 1905 5.7 6460 8 12/26/96 1804 5.6 5390 1 2 12/27/96 1753 5.5 4920 1 3 I 1 2/28/96 2633 5.6 4840 21 1 2/29/96 2617 5.6 5240 14 1 2/30/96 2772 5.7 4110 1 0 I 12/31 /96 3144 5.6 6390 3 AVG: 1899 5.6 5660 1 1 1469 I MAX: 3144 5.9 8660 31 1874 MIN: 903 5.3 3750 3 1170 I I I I I GROUNDWATER MONTHLY MONITORING: OUTER TIER COMBINED INFLUENT: #1 OTCI I PAGENO.1 DEC 1996 DATE: FLOW: PH: TOG: I GA) pH ppm 12/01/96 71905 6.1 I 1 2/02/96 72278 6.1 12/03/96 71889 6.0 4 12/04/96 72575 6.0 I 12/05/96 72092 5.9 1 2/06/96 71187 5.7 12/07/96 73700 5.7 I 12/08/96 71727 6.0 12/09/96 72089 5.8 9 I 12/1 0/96 72961 6.1 12/11/96 71718 6.1 12/12/96 70923 6.0 I 12/13/96 74818 6.1 12/14/96 71120 6.0 12/15/96 72684 5.9 I 12/16/96 72571 6.2 12/17/96 68285 6.0 7 12/18/96 55817 5.9 I 12/19/96 72745 6.3 1 2/20/96 75824 5.9 12/21/96 76487 5.7 I 1 2/22/96 72033 5.7 12/23/96 75489 6.5 12/24/96 61626 6.5 4 I 1 2/25/96 76497 5.7 12/26/96 75166 5.8 12/27/96 74934 6.5 I 12/28/96 74486 5.9 1 2/29/96 74450 5.9 12/30/96 74060 5.9 I 12/31 /96 74914 6.0 AVG: 72227 6.0 6 I MAX: 76497 6.5 9 MIN: 55817 5.7 4 I I I I I GROUNDWATER MONTHLY MONITORING: SBA MIXED LIQLOR: S8RML I PAGE N0.4 DEC 1996 SETT. SLUJGE 5/DAY DATE: PH: NH3N: P04: DO: MLSS: MLVSS: SOLIDS: WASTED F/M: F/M: pH ppm ppm ppm ppm ppm ml/I gal ratio ratio I 12/01 /96 8.2 210 29.0 3.2 2760 980 40 0.16 12/02/96 8.2 141 17.0 3.0 2612 1000 54 0.17 12/03/96 8.2 151 12.0 2.9 2888 1000 100 0.12 ,I 12/04/96 8.2 162 20.5 3.1 3044 2060 980 100 0.00 12/05/96 8.1 145 29.8 3.0 2960 990 25 0.11 0.11 12/06/96 8,0 130 40.0 3.1 2840 960 94 0.13 0.11 12/07/96 8.1 134 36.0 3.0 2960 990 202 0.00 0.07 I 12/08/96 8.3 156 13.0 3.5 2632 980 121 0.15 0.08 12/09/96 7.9 139 26.1 4.5 2500 975 220 0.16 0 .11 12/10/96 8.4 107 20.4 4.1 2588 970 100 0.00 0.09 12/11/96 8.2 64 33.2 3.6 2516 1836 980 40 0.18 0.10 I 12/12/96 8.1 163 13.0 3.5 2572 980 200 0.00 0.10 12/13/96 8,5 168 23.5 3.9 2388 960 25 0.24 0.12 1 2/14/96 8.3 163 28.0 3.2 2444 960 0 0.18 0.12 I 12/15/96 8.2 160 30.0 3.1 2752 900 25 0.00 0.12 12/16/96 8.4 212 43.6 3.0 2008 890 25 0.19 0.12 12/17/96 8.3 169 54.6 4.3 2632 940 25 0.12 0.15 12/18/96 8.3 153 22.2 4.2 2732 1416 850 40 0.21 0.14 I 12/19/96 8.3 152 28.4 5.2 2720 840 100 0.13 0.13 1 2/20/96 8.3 126 24.6 6.6 2804 800 100 0.00 0.13 12/21/96 8.2 130 25.0 4.4 3692 830 40 0.14 0.12 12/22/96 8.3 136 26.0 6.0 2880 800 54 0.17 0.13 I 1 2/23/96 8. 1 120 18.0 5.1 3268 700 0 0.00 0.09 1 2/24/96 8.0 205 36.0 6.2 2848 725 54 0.15 0.09 12/25/96 8.2 159 9.4 5.5 3476 700 54 0.15 0.12 1 2/26/96 8.3 126 8.0 5.0 3424 800 40 0.00 0.10 I 12/27/96 8.5 152 8.3 5.2 2480 900 81 0.20 0.10 12/28/96 8.4 169 20.0 5.6 3496 900 81 0.14 0.13 1 2/29/96 8.4 136 18.9 5.0 3072 950 94 0.15 0.13 1 2/30/96 8.3 106 18.0 4.3 3312 960 100 0.12 0.13 I 12/31/96 8.5 103 38.4 3.5 2440 950 54 0.14 AVG: 8.2 147 25 4 2830 1771 908 74 0.12 0.11 I MAX: 8.5 212 55 7 3692 2060 1000 220 0.24 0.15 MIN: 7.9 64 8 3 2008 1416 700 0 0.00 0.07 •• I I I I I I I GROUNDWATER MONTHLY MONITORING: AFTER PLATE SEPARATOR BEFORE SBR: SBRJ I PAGENO.3 DEC 1996 DATE: PH: COD: TSS: I' pH ppm ppm 12/01 /96 5.8 4900 20 ,I 12/02/96 6.4 5000 28 12/03/96 6.0 3950 1 6 12/04/96 I 12/05/96 6.0 3800 24 12/06/96 5.8 4310 28 12/07/96 :I 1 2/08/96 5.7 4330 44 1 2/09/96 5.7 4600 20 1 2/1 0/96 I 12/11/96 5.9 5020 36 12/12/96 12/13/96 5.7 6330 32 I ' ' 12/14/96 6.0 5000 28 1 2/15/96 I 12/16/96 5.4 4210 40 12/17/96 5.6 3640 44 12/18/96 5.7 6510 20 I 12/19/96 5.8 4020 40 1 2/20/96 12/21/96 5.9 5640 44 I 12/22/96 6.2 5660 40 1 2/23/96 12/24/96 5.9 4840 48 I, 12/25/96 6.0 6020 64 12/26/96 12/27/96 6.0 5710 84 I 12/28/96 6.0 5670 48 12/29/96 5.7 5300 44 12/30/96 6.0 4630 56 I 12/31 /96 5.6 3800 1 2 AVG: 5.9 4908 37 I MAX: 6.4 6510 84 MIN: 5.4 3640 1 2 I I I I I GROUNDWATER MONTHLY MONITORING: SBR EFFLUENT:(DECANT) #4SBRE I PAGENO.5 DEC 1996 WAS. NH3N PHOS. DATE: FLOW: COD: TSS: TSS ADDED: ADDED: I ffi) ppm ppm ppm gal lbs 12/01 /96 2219 760 200 3900 0 0 I 1 2/02/96 2501 600 420 4100 1 0 1 2/03/96 2265 555 300 4860 1 1 12/04/96 0 375 84 4200 1 1 I 12/05/96 2297 750 102 4420 0 0 12/06/96 2286 746 136 4640 0 0 12/07/96 0 710 120 5000 0 ,I 12/08/96 1997 847 860 3420 2 12/09/96 2228 11 00 860 3520 1 12/1 0/96 0 2400 2500 3440 0 0 I 12/11/96 2297 1674 2170 6100 4 0 12/12/96 0 188 160 1800 1 2 12/13/96 2239 1170 650 3480 1 1 I 12/14/96 2352 720 310 1 1 12/15/96 0 740 136 2640 1 1 .I 12/16/96 2205 648 120 2280 0 0 12/17/96 2354 594 104 3200 0 0 12/18/96 2373 621 240 2720 1 1 I 12/19/96 2466 491 200 3000 0 0 12/20/96 0 507 240 2804 1 1 12/21 /96 2151 501 228 4440 1 1 I 12/22/96 2513 480 200 4000 1 1 12/23/96 0 360 160 1 1 12/24/96 2263 461 180 4200 0 0 I 12/25/96 2408 444 184 8000 1 1 1 2/26/96 0 339 120 7000 2 2 12/27/96 1425 158 120 8020 1 2 .I 12/28/96 2321 172 84 5480 1 1 12/29/96 2369 162 156 6000 1 1 12/30/96 2173 188 68 5500 1 1 ·• 12/31/96 2380 194 340 5420 1 0 AVG: 1680 634 379 4399 1 1 I MAX: 2513 2400 2500 8020 4 2 MIN: 0 158 68 1800 0 0 I I ., I I GROUNDWATER MONTHLY MONITORING: INNER TIER EQUALIZATION TANK: ITEQT I PAGENO,2 DEC 1996 DATE: PH: COD: OT WATER ADDED I pH ppm gal 12/01 /96 7.6 4800 I 12/02/96 7.9 4400 12/03/96 7.6 4100 12/04/96 7.5 4700 I 12/05/96 8.3 4500 12/06/96 7.3 4740 12/07/96 7.4 4640 I 12/08/96 7.4 4390 12/09/96 7.8 4250 12/10/96 7.9 3750 I 12/11/96 7.2 4990 1 2/12/96 7.6 4240 'I 12/13/96 7.5 5380 12/14/96 7.4 5000 12/15/96 7.3 6220 12/16/96 7.4 4230 I 12/17/96 7.6 3640 12/18/96 7.5 5840 I 12/19/96 7.5 4140 12/20/96 12/21/96 7.7 5470 I 12/22/96 7.8 5540 12/23/96 7.5 4490 12/24/96 7.2 5310 I 12/25/96 7.4 6050 12/26/96 7.8 · 4590 12/27/96 7.4 6090 I 1 2/28/96 7.5 4540 12/29/96 7.5 5350 12/30/96 7.6 4440 I 12/31/96 7.4 4730 AVG: 7.6 4818 0 I MAX: 8.3 6220 0 MIN: 7.2 3640 0 I I I I I GROUNDWATER MONTHLY MONITORING: INNER TIER CARBON FILTER EFFWENT #8 ITEF I PAGE NO. 7 DEC 1996 DATE: PH: COD: TOG: TSS: I pH ppm ppm ppm 12/01/96 I 12/02/96 12/03/96 56 12/04/96 I 12/05/96 8.3 610 67 12/06/96 I 12/07/96 12/08/96 12/09/96 70 I 12/1 0/96 12/11/96 8.4 1570 12/12/96 I, 12/13/96 12/14/96 12/15/96 I 1 2/16/96 12/17/96 8.4 693 1 9 12/18/96 I 12/19/96 1 2/20/96 12/21/96 I 12/22/96 1 2/23/96 12/24/96 69 I 12/25/96 12/26/96 12/27/96 I 12/28/96 1 2/29/96 1 2/30/96 I 12/31 /96 AVG: 8.4 958 54 67 I MAX: 8.4 1570 70 67 MIN: 8.3 610 1 9 67 I I I I I GROUNDWATER MONTHLY MONrrORING: I OUTER TIER CARBON FILTER EFFLUENT: #7 OTEF PAGENO.3 DEC 1996 I DATE: PH: TOG: TSS: pH ppm ppm I 12/01/96 12/02/96 1 2/03/96 6 I 12/04/96 12/05/96 6.9 5 12/06/96 I 12/07/96 1 2/08/96 1 2/09/96 3 I 12/10/96 12/11/96 7.0 12/12/96 I 12/13/96 12/14/96 12/15/96 I 12/16/96 12/17/96 7.5 3 1 2/1 8/96 I 12/19/96 1 2/20/96 12/21 /96 •· 12/22/96 12/23/96 12/24/96 3 3 I 12/25/96 12/26/96 12/27/96 I 12/28/96 1 2/29/96 1 2/30/96 I 12/31/96 AVG: 7.1 4 4 I MAX: 7.5 6 5 MIN: 6.9 3 3 I ·I I I I GROUNDWATER MONTHLY MONITOF I RAINFALL DATA I DATE INCHES/DAY I 12/01/96 1.20 12/02/96 0.00 1 2/03/96 0.00 I 12/04/96 0.00 1 2/05/96 0.60 12/06/96 0.00 I 1 2/07 /96 0.60 12/08/96 0.00 1 2/09/96 0.00 I 12/1 0/96 0.00 12/11/96 0.00 1 2/12/96 1.00 I 12/13/96 0.00 12/14/96 0.00 12/15/96 0.00 I 12/16/96 0.30 12/17/96 1.00 1 2/1 8/96 0.90 I 12/19/96 0.00 1 2/20/96 0.00 12/21/96 0.00 I 12/22/96 0.00 12/23/96 0.00 12/24/96 0.20 I 12/25/96 0.00 12/26/96 0.00 12/27/96 0.00 I 12/28/96 0.20 12/29/96 0.00 1 2/30/96 0.00 I 12/31/96 0.00 TOTAL 6 •• I I I I I I I I I I I I I I I I I I I I I I MAINTENANCE ACTIVITIE&GROUNDWATER OPEAABlE UNIT #1 NNER TIER SYSTEM DATE LOCATION 12/03196 IT-9 12/21196 IT-5 PAC:a.EM LOW FLOW LOW FLOW ACTlON DATE 12113196 12121196 ACTlON CLEANED PROBES CHANGED Ell.ADDER, CLEANED SCREEN MECHANIC JPPP JPPP I I I I I I I I I I I I I I I I I I I MAINTENANCE ACTIVITIE&GROUNDWATER OPERABLE UNIT #1 OUTER TIER SYSTEM DATE LOCATION PRCB.EM 11/04/96 OT-6A LOW FLOW 1 0/09/96 OT-2 LOW FLOW 11/13/96 OT-6A NOR.OW 11/22/96 OT-6 LEAK 12/16/96 OT-5 LOW FLOW ACTIOO DATE 11/05/96 11 /05/96 11/14/96 11 /22/96 ACTIOO SET FLOW TO 7.5 GPM REPLACED Bl.ADDER CLEANED SCREEN REPLACED FLOW METER REPLACED FLOW SWITCH MECH/>NIC PPJP JPPP ,PPJP RAPP I I I I I I I I I I I I I I I I I I I Attachment 2 QA Summary Report and Analytical Data for the July 11-12, 1996 Sampling Event I I I I I I I I I I I I I I I I I I I DAT A ASSESSMENT CHECKLIST REPORT . LEVEL II Client ID: Hoechst-Celanese/Shelby Prepared by: &Sil Sample Delivery Group (SDG) Description: Project Number: Date: TF026TS05 WJ!)f}_ 3rd qµarter 1996 monitoring samples collected and analyzed by Shealy Enyjronmental Laboratories for volatiles, TOC and ethylene ~yco! according to the sampljng and analysis plan dated fone 96 CONTENTS LEVEL COMMENTS II Sample Results ✓ All data Class A Method Conformance Summary ✓ Satisfactory Chain(s) of Custody (COCs) ✓ Client and project contact information incomplete (no effect on data) Master Tracking List ✓ Satisfactory Case Narrative Sample Prep Standards Prep Instrument Quality Control Data Batch Quality Control Report Surrogate Recovery Report Trip/Field/Equipment Blank Report ✓ Satisfactory Field Notes/Logbook ✓ Satisfactory CLP Forms All Raw Data Electronic Deliverables ✓ Satisfactory Discussion: For the DQOs of this project (level II) to be met, the data was assessed based on reported method non-conformances and the following overall project criteria: • holding times • completeness • blank contamination • transcription accuracy • report qualifiers • comparability/consistency with historical data Class A = quantitative Class B = qualitative Class C = unusable Kubal-Furr & Associates a I I I I I I I I I I I I I I I I I I HOECHST CELANESE Shelby, NC ANALYTICAL DATA PACKAGE Third Quarter 1996 (ii:)f?nll. . . - \ JUL 3 1 1996 1 ; I L.. -L'.5 _____ · _____ ------------ Data package provided by: SHEALY ENVIRONMENT AL SERVICES, INC. 106 Vantage Point Drive Overlook Business Center Cayce, SC 29033 (803)791-9700 m m I I I I I I I I I I I I I I I I I TABLE OF CONTENTS I. Master Tracking List II. Sample Results (By analytical test method) III. Method Conformance Summary IV. Field Data Summary V. Chain of Custody Records I I I I I I I I I I I I I I I I I I I MASTER TRACKING LIST .. ------------------~ Client Sample Identification ITCI ITEF OTCI OTEF . C-49 K-28 P-58 T-35 V-23 AA-54 AA-54(a) CC-33 EE-58 FF-34 FF-62 GG-61 HH-48 HH-77 Master Tracking List HOECHST CELANESE-Shelby Third Quarter 1996 SHEALY Lab Date ID Number Collected Ground-Water 92684 07/12/96 92685 07/12/96 92686 07/12/96 92687 07/12/96 92690 07/12/96 92672 07/11/96 92673 07/11/96 92688 07/12/96 92671 07/11/96 92679 07/12/96 92679A 07/12/96 · 92694 07/12/96 92683 07/12/96 92681 07/12/96 92682 07/12/96 92680 07/12/96 92691 07/12/96 92692 07/12/96 Date Received 07/15/96 07/15/96 07/15/96 07/15/96 07/15/96 07/15/96 07/15/96 07/15/96 07/15/96 07/15/96 07/15/96 07/15/96 07/15/96 07/15/96 07/15/96 07/15/96 07/15/96 07/15/96 u m I I I SAMPLE RESULTS I Total Organic Carbon (TOC) I Method 415.1 I I I I I I I I I I I I - - - - - - - - - - - - - - - -iiiiiil iiiiil ;;;; Client Sample · Identification ITCI ITEF K-28 V-23 Master Tracking List -TOC HOECHST CELANESE-Shelby Third Quarter 1996 SHEALY Lab Date Date ID Number Collected Received 92684 07/12/96 07/15/96 92685 07/12/96 07/15/96 92672 07/12/96 07/15/96 92671 07/12/96 07/15/96 Analysis Date 07/22/96 07/26/96 07/22/96 07/22/96 SHEALY ENVIRONMENTAL SERVICES, INC. I Scientists and Consultants 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS (803) 791-9700 FAX (803) 791-9111 I SC DHEC No. 32010 Client: I Attention: I SHEALY Lab No, 92684 Description: ITCI Date Received: 07/15/96 I Date Reported, 07/23/96 I I I I I I I I I I I I I Parameters INORGANICS TOC TOC Duplicate HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method 415.1 415.1 Result 2600 2400 Units mg/1 mg/1 Terms and Conditions on Reverse Side NC DEHNR No. 329 Coll. Date: 07/12/96 Coll. Time: 1045 QA/QC Officer 9& J?evrr!tk7 V.P. Analytical __ !"._;;,,/ ___ _ Date Date PQL Prepared Analyzed Anal. 1.0 07/22/96 MLK 1.0 07/22/96 MLK I I I I I I I I I I I I I I I I I I 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 SC DHEC No. 32010 Client: Attention: SHEALY Lab No, 92685 Description: ITEF Date Received: 07/15/96 Date Reported: 07/24/96 Parameters INORGANICS TOC TOC Duplicate SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 07/12/96 Coll. Time: 1055 QA/QC Officer 9JinJJw/ll,dE V.P. Analytical --~M~:~--- Date Date Method Result Units POL Prepared Analyzed Anal. 415.1 415.1 130 120 mg/l mg/1 Terms and Conditions on Reverse Side 1.0 07/26/96 JYR 1.0 07/26/96 JYR I I I I I I I I I I I I I I I I I I 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 SC DHEC No. 32010 Client: Attention: SHEALY Lab No, 92672 Description: K-28 Date Received: 07/15/96 Date Reported: 07/23/96 Parameters INORGANICS TOC TOC Duplicate SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 07/11/96 Coll. Time: 1657 Qriofw),rn()f V.P. Analytical --'/))C!Ll8'.':::::'.'.'.,_ __ _ QA/QC Officer Date Date Method Result Units PQL Prepared Analyzed Anal. 415.1 415.1 17 17 mg/1 mg/1 Terms and Conditions on Reverse Side 1.0 07/22/96 MLK 1.0 07/22/96 MLK 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 I SC DHEC No. 32010 Client: I Attention: I SHEALY Lab No, 92671 Description: V-23 Date Received: 07/15/96 I Date Reported, 07/23/96 I Parameters INORGANICS TOC Duplicate I TOC I I I I I I I I I I I SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 07/11/96 Coll. Time: 1625 QA/QC Officer QAD /lo¥ mo 1; r,: 0 J V.P. Analytical-~~-~---- Date Date Method Result units PQL Prepared Analyzed Anal. 415.1 415.1 10400 11000 mg/1 mg/1 Terms and Conditions on Reverse Side 1.0 1.0 07 /22/96 MLK 07/22/96 MLK g 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 I SC DHEC No. 32010 Client: I Attention: SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 I SHEALY Lab No, 92678 Description: Precleaned Equipment Blank Coll. Date: 07/11/96 Coll. Time: 1620 Date Received: 07/15/96 I Date Reported, 07 /24/96 I Parameters INORGANICS I TOC TOC Duplicate I I I I I I I I I I I Method 415.1 415.1 Result ND ND Units mg/1 mg/1 Terms and Conditions on Reverse Side QA/QC Officer <i)~Qj!}/1tJG' V.P. Analytical---~~--- Date Date PQL Prepared Analyzed Anal. 1.0 07/22/96 MLK 1.0 07/22/96 MLK I 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 I SC DHEC No. 32010 Client: I Attention: SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 I SHEALY Lab No, 92689 Description: Precleaned Equipment Blank Coll. Date: 07/12/96 Coll. Time: 1200 Date Received: 07/15/96 I Date Reported, 07 /23/96 I Parameters INORGANICS I TOC TOC Duplicata I I I I I I I I I I I Method 415.1 415.1 Result ND ND Units mg/1 mg/1 Terms and Conditions on Reverse Side ~ MJ..lmoc:=: V.P. Analytical -~/Yl=,},<,/ ___ _ QA/QC Officer Date Date PQL Prepared Analyzed Anal. 1.0 07/22/96 MLK 1.0 07/22/96 MLK g m • I SAMPLE RESULTS I I Ethylene Glycol I Method 8015A I I I I I I I I I I I I - - - - - - - - - - - - - --liiil iiii iiiii -- Client Sample Identification ITCI ITEF Master Tracking List -Ethylene Glycol HOECHST CELANESE-Shelby Third Quarter 1996 SHEALY Lab Date Date · ID Number Collected Received 92684 07/12/96 07/15/96 92685 07/12/96 07/15/96 Prep. Analysis Date Date 07/16/96 07/17/96 07/16/96 07/17/96 D 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 I SC DHEC No. 32010 Client: I Attention: I SHEALY Lab No: 92085 Description: ITEF Date Received: O?_l,~5/96 I Date Reported, 07/24/96 I I I .I I I I I I I I I I Parameters Ethylene glycol SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 07/12/96 Coll. Time: 1055 QA/QC Officer ~1(;:rJf'ntJi v. P. Analytical fu /h--"' Date Date Method Result Units PQL Prepared Analyzed Anal. 8015A ND mg/1 6.5 07/16/96 07/17/96 SAG Terms and Conditions on Reverse Side I I 1 06 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 SC DHEC No. 32010 Client: Attention: . -.-• SHEALY Lab No, 92684 _g; Description: ITCI I Date Received: 07/15/96 Date Reported: 07/23/96 I• Parameters Ethylene glycol I· I I I 11 ,, ,, I I I I I I SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 07/12/96 Coll. Time: 1045 QA/QC Officer V. P. Analytical Date Date Method Result Units PQL Prepared Analyzed Anal. 8015A 550 mg/l 6_5 07/16/96 07/17/96 SAG Terms and Conditions on Reverse Side I t I I I i SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS (803) 791-9700 FAX (803) 791-9111 SC DHEC No. 32010 Client: Attention: SHEALY Lab No, 92689 HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank NC DEHNR No. 329 Description: Precleaned Equipment Blank Coll. Date: 07/12/96 Coll. Time: 1200 Date Received: 07/15/96 Date Reported: 07/23/96 Parameters Method Result Units Ethylene glycol 8015A ND mg/1 Terms and Conditions on Reverse Side PQL QA/QC Officer V.P. Analytical Date Date Prepared Analyzed Anal. 6.5 07/16/96 07/17/96 SAG I I I 1· ff, I, ·t. I I .11 1· ,I ,, I I ·I I I I SAMPLE RESULTS TCL Volatiles Method 8260A Client Sample Identification ITCI ITEF OTCI OTEF C-49 K-28 P-58 T-35 V-23 AA-54 AA-54(a) CC-33 EE-58 FF-34 FF-62 GG-61 HH-48 HH-77 Master Tracking List -TCL VOCs HOECHST CELANESE-Shelby Third Quarter 1996 SHEALY Lab Date Date ID Number Collected Received 92684 07/12/96 07/15/96 92685 07/12/96 07/15/96 92686 07/12/96 07/15/96 92687 07/12/96 07/15/96 92690 07/12/96 07/15/96 92672 07/11/96 07/15/96 92673 07/11/96 07/15/96 92688 07/12/96 07/15/96 92671 07/11/96 07/15/96 92679 07/12/96 07/15/96 92679A 07/12/96 07/15/96 92694 07/12/96 07/15/96 92683 07/12/96 07/15/96 92681 07/12/96 07/15/96 92682 07/12/96 07/15/96 92680 07/12/96 07/15/96 92691 07/12/96 07/15/96 92692 07/12/96 07/15/96 Analysis Date 07/22/96 07/18/96 07/19/96 07/19/96 07/19/96 07/18/96 07/18/96 07/19/96 07/19/96 07/18/96 07/24/96 07/22/96 07/19/96 07/18/96 07/18/96 07/18/96 07/19/96 07/19/96 I 1 06 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 ,I· SC DHEC No. 32010 I I I I Client: Attention: SHEALY Lab No, 92684 Description: ITCI Date Received: 07/15/96 Date Reported: 07/24/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromometbane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trane-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 2-hexanone methylene chloride 4-methyl-2-pentanone styrene 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenes SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result Units PQL 8260A 0.6210 mg/1 0.0200 8260A 0.0512 mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A 0. 097 9 mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A 0.0401 mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A 0.1330 mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side QA/QC (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 07 /12/96 Coll. Time: 1045 Officer 9-,,( () li~/7 !lit':; I , V.P. Analytical /t:1 k::::::'. Date Date Prepared Analyzed Anal. 07/22/96 SAG SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS (803) 791-9700 FAX (803) 791-9111 SC DHEC No. 32010 Client: Attention: I SHEALY Lab No, 92685 1 , Description: ITEF Date ,, Date Received: 07/15/96 Reported: 07/24/96 11• Parameters ORGANICS , acetone :1 VOLATILE benzene bromodichloromethane I bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride ' .• -·-' chlorobenzene chloroethane chloroform chloromethane dibromochloromethane ,,. 1, 1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene I~ trans-1,2-dichloroethene , ' 1, 2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ~ ethylbenzene I 2-hexanone · 1 methylene chloride ~ 4-methyl-2-pentanone styrene ·1·, l, l, 2, 2-tetrachloroethane tetrachloroethene toluene l,1,1-trichloroethane I 1 I, 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenee HOECHST CELANESE-SHELBY P.O. Box 87 PLANT Shelby, NC 28151-0087 Kathryn Frank Method Result Unite PQL 8260A ND mg/1 0.0200 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side NC DEHNR No. 329 Coll. Date: 07 /12/96 Coll: Time: 1055 QA/QC Officer {J<M!6o-J!)tJ[ V.P. Analytical Mfr-v' Date Date Prepared Analyzed Anal. 07/18/96 SAG I I ,I I ,, 'I I I I 1· I SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS SC DHEC No. 32010 Client: Attention: SHEALY Lab No, 92686 Description: OTCI Date Received: 07/15/96 Date Reported: 07/23/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 2-hexanone methylene chloride 4-methyl-2-pentanone styrene 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenes HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result Units PQL 8260A ND mg/1 0.0200 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side QA/QC (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 07/12/96 Coll. Time: 1105 Officer V.P. Analytical ~noF Date Date Prepared Analyzed Anal. 07/19/96 SAG I I .1 I ,, I I I I· u 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 SC DHEC No. 32010 Client: Attention: SHEALY Lab No: 92687 Description: OTEF Date Received: 07/15/96 Date Reported: 07/23/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cie-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 2-hexanone methylene chloride 4-methyl-2-pentanone styrene 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenes SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method 8260A 8260A 8260A 8260A 8:Z60A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8~60A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Units mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 Terms and Conditions on Reverse Side PQL 0.0200 0.0050 0.0050 0,0050 0.0100 0.0050 0.0050 0.0050 0.0050 0.0100 0.0050 0.0100 0.0050 0.0050 0,0050 0.0050 0.0050 0.0050 0,0050 0.0050 0.0050 0.0050 0.0050 0.0050 0,0050 0,0050 0.0050 0.0050 0.0050 0.0050 0.0050 0,0050 0.0050 0.0100 0.0150 (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 07/12/96 Coll. Time: 1110 QA/QC Officer V.P. Analytical Date Date Prepared Analyzed Anal. 07/19/96 SAG I I I I ,, I I ,, 1 I I I SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS SC DHEC No. 32010 Client: Attention: SHEALY Lab No, 92690 Description: C-49 Date Received: 07/15/96 Date Reported: 07/23/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride. chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 2-hexanone methylene chloride 4-methyl-2-pentanone styrene 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenes HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result Units PQL 8260A ND mg/1 0.0200 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side QA/QC (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 07/12/96 Coll. Time: 1225 Officer 9i1-(1 ©Vl2/JF. V. P. Analytical M& Date Date Prepared Analyzed Anal. 07/19/96 SAG I SHEALY ENVIRONMENTAL SERVICES, INC. I Scientists and Consultants 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS (803) 791-9700 FAX (803) 791-9111 .I SC DHEC No. 32010 Client: I Attention: I. SHEALY Lab No, 92672 , Description: K-28 I •• I I I I 0 I I Date Received: 07/15/96 Date Reported: 07/23/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 2-hexanone methylene chloride 4-methyl-2-pentanone styrene 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenes HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result Units PQL 8260A ND mg/1 0.0200 8:Z60A 0.0149 mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8:.260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side NC DEHNR No. 329 Coll. Date: 07 /11/96 Coll. Time: 1657 QA/QC Officer <J<,-0 ( vv(Y)l)t; V. P. Analytical Mk-/ Date Date Prepared Analyzed Anal. 07/18/96 SAG I SHEALY ENVIRONMENTAL SERVICES, INC. 1 Scientists and Consultants 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA29033 CERTIFICATE OF ANALYSIS (803) 791-9700 FAX (803) 791-9111 I SC DHEC No. 32010 Client: I Attention: I SHEALY Lab No: 92673 Description: P-58 Date Received: 07/15/96 I Date Reported: 07/23/96 I Parameters •• VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform .I bromomethane 2-butanone carbon disulfide carbon tetrachloride I chlorobenzene chloroethane chloroform chloromethane dibromochloromethane I 1,1-dichloroethane . 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene U trans-1,2-dichloroethene 1,2-dichloropropane 1 cis-1, 3-dichloropropene trans-1,3-dichloropropene ethylbenzene fl 2-hexanone 11· methylene chloride 4-methyl-2-pentanone styrene I, 1,1,2,2-tetrachloroethane tetrachloroethene '_ ' toluene 1,1,1-trichloroethane 1,1,2-trichloroethane I trichloroethene ' vinyl acetate vinyl chloride xylenes I I I HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result Units PQL 8260A ND mg/1 0.0200 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050· 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 l: 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0,0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side NC DEHNR No. 329 Coll. Date: 07 /11/96 Coll. Time: 1727 QA/QC Officer 9":)t)m~~ V.P. Analytical Date Date Prepared Analyzed Anal. 07/18/96 SAG I I I I I I I I I ,, I I, D I 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 SC DHEC No. 32010 Client: Attention: SHEALY Lab No: 92688 Description:. T-35 Date Received: 07/15/96 Date Reported: 07/23/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 2-hexanone methylene chloride 4-methyl-2-pentanone styrene 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1 1,1,2-trichloroethane trichloroethene ·vinyl acetate vinyl chloride xylenes I I I SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result Units POL 8260A ND mg/1 0.0200 8260A ND mg/1 0.0050 8:260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side QA/QC (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 07/12/96 Coll. Time: 1140 Officer ~·u 1/r;c:"//ltJf C, V.P. Analytical lyJJ:v::: Date Date Prepared Analyzed Anal. 07/19/96 SAG I I I I I I I I I I I g fl I I I I 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 SC DHEC No. 32010 Client: Attention: SHEALY Lab No: 92671 Description: v-23 Date Received: 07/15/96 Date Reported: 07 /23/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 2-hexanone methylene chloride 4-methyl-2-pentanone styrene 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenes SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result Units PQL 8260A 1.1500 mg/1 0.0200 8260A 0.0291 mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A 0.5040 mg/1 0.0050 8260A 0.0591 mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND. mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0,0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A 0.3430 mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0,0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A 0.0065 mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0,0050 8260A ND mg/1 0.0050 8260A ·ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side QA/QC (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 07 /11/96 Coll. Time: 1625 Officer ~ #,DJ\, mv1,;_- V.P. Analytical ;V'1 .I}---- Date Date Prepared Analyzed Anal. 07/19/96 SAG I I I I I I I I I I I I I g I I I I I 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 SC DHEC No. 32010 Client: Attention: SHEALY Lab No: 92679 Description: AA-54 Date Received: 07/15/96 Date Reported: 07/23/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cie-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 2-hexanone methylene chloride 4-methyl-2-pentanone styrene 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenes SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result Units PQL 8260A ND mg/1 0.0200 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side QA/QC (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 07 /12/96 Coll. Time: 0752 Officer 9 ,. ;J, ~. f'.\<) oJ,71 t" u V.P. Analytical r,,,V Date Date Prepared Analyzed Anal. 07/18/96 SAG I I I I I I I I I I I I 0 m I I I I I SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants 1 06 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS (803) 791-9700 FAX (803) 791-9111 SC DHEC No. 32010 Client: Attention: SHEALY Lab No: 92679A Description: AA-54 (al Date Received: 07/15/96 Date Reported: 07/26/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 2-hexanone methylene chloride 4-methyl-2-pentanone styrene 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenes HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result units PQL 8260A ND mg/1 0.0200 8260A ND mg/1 o.ooso 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side NC DEHNR No. 329 Coll. Date: 07/12/96 Coll. Time: 0752 QA/QC Officer J<i,J t!o_AJtr1ue V.P. Analytical ~ /Vt Date Date Prepared Analyzed Anal. 07/24/96 SAG I I 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 I SC DHEC No. 32010 I I I I I I I I I I I I I I Client: Attention: SHEALY Lab No, 92694 Description: CC-33 Date Received: 07/15/96 Date Reported: 07/23/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 2-hexanone methylene chloride 4-methyl-2-pentanone styrene 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenee SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result units PQL 8260A ND mg/1 0.0200 8260A 0.0128 mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0200 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0_0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side QA/QC (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 07 /12/96 Coll. Time: 1040 Officer V. P. Analytical Date Date Prepared Analyzed Anal. 07/22/96 SAG I I I I I I I I I I I I I I I I I I I SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS (803) 791-9700 FAX (803) 791-9111 SC DHEC No. 32010 Client: Attention: SHEALY Lab No: 92683 Description: EE-58 Date Received: 07/15/96 Date Reported: 07/23/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 2-hexanone methylene chloride 4-methyl-2-pentanone styrene 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenee HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result Unite PQL 8260A ND mg/1 0.0200 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/l 0.0050 8260A ND mg/1 0.0050 8260A ND mg/l 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/l 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/l 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side NC DEHNR No. 329 Coll. Date: 07/12/96 Coll. Time: 1000 QA/QC Officer <;_)i,.J f/(A;}//)(: V. P. Analytical I fVlrfJ Date Date Prepared Analyzed Anal. 07/19/96 SAG I I I I I I I I I I I I I I I I I I I 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 SC DHEC No. 32010 Client: Attention: SHEALY Lab No: 92681 Description: PP-34 Date Received: 07/15/96 Date Reported: 07/23/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 2-hexanone methylene chloride 4-methyl-2-pentanone styrene l,l,2,2•tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenee SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result Units PQL 8260A ND mg/1 0.0200 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side QA/QC (803) 791-9700 FAX (803) 791 ·9111 NC DEHNR No. 329 Coll. Date: 07/12/96 Coll. Time: 0850 Officer V.P. Analytical 9i1:) 1'70(: /VI Date Date Prepared Analyzed Anal. 07/18/96 SAG I I I 06 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 I SC DHEC No. 32010 Client: I Attention: I SHEALY Lab No, 92682 Description: FF-62 Date Received: 07/15/96 Reported: 07/23/96 I Date I Parameters I VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform I bromomethane 2-butanone carbon disulfide carbon tetrachloride I chlorobenzene chloroethane chloroform chloromethane dibromochloromethane I 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cie-1,2-dichloroethene I trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 12 -hexanone methylene chloride 4-methyl-2-pentanone styrene I 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane I trichloroethene vinyl acetate vinyl chloride xylenes I I I I SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result Units PQL 8260A ND mg/1 0.0200 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side QA/QC (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 07/12/96 Coll. Time: 0910 Officer (Jcl,{1-[fk-, ff} !)E v.P. Analytical MV ' Date Date Prepared Analyzed Anal. 07/18/96 SAG I SHEALY ENVIRONMENTAL SERVICES, INC. I Scientists and Consultants 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS (803) 791-9700 FAX (803) 791-9111 I SC DHEC No. 32010 I I I I I I I I I I I I I I I I Client: Attention: SHEALY Lab No, 92680 Description: GG-61 Date Received: 07/15/96 Date Reported: 07/23/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibro!JlOChloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 2-hexanone methylene chloride 4-methyl-2-pentanone styrene 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenes HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result Units PQL 8260A ND mg/1 0.0200 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0,0050 8260.A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side NC DEHNR No. 329 Coll. Date: 07 /12/96 Coll. Time: 0831 QA/QC Officer 9M f;,,,1,,i:!.J1Ji.? [) V.P. Analytical Mc~ Date Date Prepared Analyzed Anal. 07/18/96 SAG I I 106 VANTAGE POINT DRIVE CAYCE. SOUTH CAROLINA 29033 I SC DHEC No. 32010 I I I I I I I I I I I I I I I I Client: Attention: SHEALY Lab No, 92691 Description: HH-48 Date Received: 07/15/96 Date Reported: 07/23/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trane-1,3-dichloropropene ethylbenzene 2-hexanone methylene chloride 4-methyl-2-pentanone styrene 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenes SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result unite PQL 8260A ND mg/1 0.0200 8260A ND mg/1 0.0050 8:260A ND mg/1 0.0050 8:260A ND mg/1 0.0050 8:260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A 0.1790 mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side QA/QC (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 07/12/96 Coll. Time: 1300 Officer I ~ /} "' ,, ll'ic,t-;- V.P. Analytical Mfr!! Date Date Prepared Analyzed Anal. 07/19/96 SAG I SHEALY ENVIRONMENTAL SERVICES, INC. I Scientists and Consultants 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS (603) 791-9700 FAX (603) 791-9111 I SC DHEC No. 32010 I I I I I I I I I I I I I I I I Client: Attention: SHEALY Lab No, 92692 Description: HH-77 Date Received: 07/15/96 Date Reported: 07/23/96 Parameters VOLATILE ORGANICS acetone benzene bromodichlorometh~ne bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 2-hexanone methylene chloride 4-methyl-2-pentanone styrene 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,l-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenes HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result Units PQL 8260A ND mg/1 0.0200 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0,0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0,0100 8260A ND mg/1 0.0050 8260A ND mg/1 0,0100 8260A ND mg/1 0.0050 8260A ND mg/1 0,0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0,0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0,0050 8260A ND mg/1 0.0050 8260.A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0,0050 8260A 0,3830 mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side NC DEHNR No. 329 Coll. Date: 07 /12/96 Coll. Time: 1330 QA/QC Officer 9zi.o I {)1 /7'l J{3 ' (/ V.P. Analytical ('\~ Date Date Prepared Analyzed Anal. 07/19/96 SAG I SHEALY ENVIRONMENTAL SERVICES, INC. I Scientists and Consultants 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS I SC DHEC No. 32010 I I I I I I I I I Client: Attention: SHEALY Lab No, 92693TB Description: Trip Blank Date Received: 07/15/96 Date Reported: 07/23/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cie-1,2-dichloroethene trane-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dicbloropropene ethylbenzene I 2 -hexanone methylene chloride 4-methyl-2-pentanone styrene I I I I I I 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenes HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result units PQL 8260A ND mg/1 0.0200 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side QA/QC (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 07/10/96 Coll. Time: 1130 Officer 9-J.,c f(),l,;11J1/f V.P. Analytical M~ Date Date Prepared Analyzed Anal. 07/18/96 SAG I SHEALY ENVIRONMENTAL SERVICES, INC. I Scientists and Consultants 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS I SC DHEC No. Client: I Attention: 32010 HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank I SHEALY Lab No, 92678 Description: Precleaned Equipment Blank I Date Received: 07/15/96 Date Reported: 07/24/96 I Parameters I I I VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane I 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene I trans-!, 2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene I 2-hexanone methylene chloride 4-methyl-2-pentanone styrene I I I I I I 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethane vinyl acetate vinyl chloride xylenes Method 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Units mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 Terms and Conditions on Reverse Side PQL 0.0200 0.0050 0.0050 0.0050 0.0100 0.0050 0.0050 0.0050 0.0050 0.0100 0.0050 0.0100 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0100 0.0150 QA/QC (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 07 /11/96 Coll. Time: 1620 Officer V.P. Analytical 9°'~%300,; Date Date Prepared Analyzed Anal. 07/18/96 SAG I I I I I I I I I I I I I I I I I I I SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS SC DHEC No. 32010 Client: Attention: SHEALY Lab No, 92689 HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Description: Precleaned Equipment Blank Date Received: 07/15/96 Date Reported: 07/23/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloriC:a·,_ chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloroprcpene trans-1,3-dichloropropene ethylbenzene 2-hexanone methylene chloride 4-methyl-2-pentanone styrene 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenes Method 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A 8260A Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Units mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 Terms and Conditions on Reverse Side PQL 0.0200 0.0050 0.0050 0.0050 0.0100 0.0050 0.0050 0.0050 0.0050 0.0100 0.0050 0.0100 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0050 0.0100 0.0150 (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Coll. QA/QC Officer V.P. Analytical Date Date Date: 07/12/96 Time: 1200 9/.,0 /911111Ji; MV Prepared Analyzed Anal. 07/19/96 SAG I . I I I I I I I I I I I I I I I I I I METHOD CONFORMANCE SUMMARY I I I I I I I I I I I I I I I I I I I Method Conformance Summary Criteria Volatiles Ethylene Glvcol Sample Holding Time / ✓ Standards Preparation ✓ ✓ Instrument Tuning ✓ t-J/A- Instrument Calibration ✓ / Calibration Verification ,/ / Degradation Check rJ//!r N Iii- Interference Sample/Standard rJ /A-t-"lt'r Blank Results ✓ / Method Accuracy ./ I Method Precision ✓ / Surrogate Recovery ✓ µ/{t PDS/SD/MSA tJAe. I rJ//t- TCLPPrep f'J I ft !J/A Key: ✓ = Method Criteria Met N/ A = Not Applicable * = Method Criteria Not Met -see footnote(s) PDS = Post Digestion Spike · SD = Serial Dilution MSA = Method of Standard Additions Not .. I: V,)ltt+:1.._ 1XL.+.~..._~·- 'lJ..i.11 -i'./1 l\;J.b'l l -I', '1 'l-.C/0--I'. "j 10 c.. I) ; \ "'+,<; .. s '· . ,._ ~ 'i :l'-·1 t -I: l'l'l1 G) 1/v,,U. il (,,'l.'i -I\ l"i'i'l 'l)..<..'l:).-j',j 9}.(.'85-i'.<i4 Inorganics (TOC) ✓ ./ t.J//t ,/ ✓ rJ/A ,J/(\ ./ ✓ ,/ NIA Ald-e. }- N//'I I I I I I I I I I I I I I I I I I I I lHeasured bya,\t' <Jl i U.l.~ Monitoring Measuring Location Point Elevation (ft/ms!) A-39 823.36 B-34 790.62 C-49 864.11 D-27 845.50 D-35 845.69 D-56 845.19 D-88 845.52 F-55 849.19 G-50 848.48 G-88 848.26 H-59 845.25 H-79 846.53 l-57 837.63 J-29 825.18 J-59 825.01 K-28 811.20 K-58 811.39 M-28 806.72 M-44 806.71 N-29 803.38 N-53 803.82 0-25 807.54 0-59 806.61 P-31 790.00 P-58 788.12 Hoechst Celanese -Shelby, NC Water Level Measurements Page:_L of ___i Measurement Device: Electronic Water Level Indicator Depth to Water Level Comments Water Elevation (ft) (ft,msl) \~LS1-601-49 15, o'i' T:/5. 5~ [-5. 5b 3 '-I 'o . l.. I .,r:<-'' ~ \'.'.1.,v 92-'o. 4Q 1,.5e, '52 'cl .. I I 1(-,~6 62..'o.2-l , •. 7,\o '52..'o. I fe 51.e·1 -=191. 31. ·.z,-s. q9 Bo9. 4'1 c /'fut >u(,., ~sz.c, :e.·" J[ '5'0 '2,"Z. la . Co '8 41-'35 , 803.L\:0 54.80 1"11 -:f s :,\.;}..() <oor.13 21.15" '6c'-l-.(3 22. 2~ 'e>o J.. 7 \q /la. 'l j "'.f9'-t. l.f '2 1i. J . .'-t +9">.. 15 2)0. /'f T+'-.56 ')_</.~ I ' .l ~~~~---:rn. 1..r... ' I --..... ,. ...... I G\. r~.co ,qo. 30 ,i:.10 "786.4"2 1t..f,wS-"'.t92.S9 l),lt) -=t9 3. l 'o :)..2 .1.:, ~ 7(,,1. ~1- ~ ';)..t-Jc-r 7-6S: G,3, I I I I I I I I I I I I I I I I I I I Hoechst Celanese -Shelby, NC Water Level Measurements Date: II J::u 1::-i 9 '-<> Measured by: "'-<?'-£ tv'\.L\L Monitoring Measuring Depth to Location Point Water Elevation (ft) (ft/msO Q-33 783.48 21.95" R-17 779.31 Is .z..5" R-42 778.81 II .9?.. S-50 826.02 24-YS° T-17 777.90 I '-f . ':,-0 T-35 777.38 (?,.9 I T-58 776.03 [9-35" U-38 826.55 .:21-SD V-23 811.89 /'-t-9 0 W-23 800.91 I~-!o:S X-32 796.96 (>-7-~ Y-38 794.52 (?-,01 Y-74 794.87 /C,.(o:5" Z-78 797.08 '? 2-0 5'° AA-41 783.68 5'--{.'o'o AA-54 782.16 33_ l-l., BB-16 771.75 i"c 2,'2, CC-33 812.68 22-2 (o CC-64 811.37 19, 1-3 DD-58 . 796.10 33.~5" EE-58 794.48 31"-97- FF-23 772.33 /1-'Stf FF-34 772.73 iJ.-'?'-/ FF-62 772.19 {'-/.{2 Page:..l._ of -4 Measurement Device: Electronic Water Level Indicator Water Level Comments Elevation (ft,msl) -=1(.0, 53 ;, <,, <,,.o \,, 1Co (M B9 c:,,..,,_s-:, 7<-'1. i.-::i t63. t/9 . "?-5,. <,e, 8 ~ o,;- ?-'f<o. 'l'1 -.,.p,s-.2S -=r8l. 2.1 1'1(,, . 't 13 ":+1R. 22 7 7!,. 03 ~ --. .,.,.... t ... 1-'/'c,. 80 7'f 8.Lt u -:i-ta 3. e-::i- "1't 6. Lf 2 '1Cf(. /,,'-f -:Z(ol. 1-5 '.:1,:,5. G, ( v,1p.r0Z... f~(:71,.)\Z",;?'t"" vJG-.>--Cf½\NI.." (,,,-.IO Gl'-"«.-o :/-5"/. './-'1 ~5'=1. P/1 I I l"M'Z""r? Or-.... • ":"t'°:"k \ W €L..\.... GW:,1rl \:'} )...t..J 0 p ".+-51-. /,, 7- I I I I I I I I I I I I I I I I I ~7~b I Hoechst Celanese -Shelby, NC Water Level Measurements Page:_]_ of ...A Measured by: M Vy , !Jlt.-j:'.. Measurement Device: Electronic Water Level Indicator Monitoring Measuring Depth to Water Level Comments Location Point Water Elevation Elevation (ft) (ft,msO (ft/msO GG-25 771.64 20. 34 151. 5 0 GG-39 770.44 19.~~ "'.l"-1. oro GG-61 771.78 2(.."1-0 "t-'-lS°. 0~ ·llll-48 755.44 . . ."< ~-'2,S' +11. ,"I llll-77 755.87 -;z_ <;/. ?, 0 711-. 5f PZ-1 773.99 I 'o-::l'-l •55. <.. u PZ-2 795.81 50,t./-1. -:/4S. 39 PZ-3 786.62 Well destroyed/Paved over between 8/95 and 11/95 PZ-4 750.07 :3. 9 Cf--=l-4fo. I o PZ-SA 788.72 "3'-1-6 <., -:, 5 4 -:a. '° PZ-SB 777.59 2fi'-e,1 <'S-1. t'o PZ-6A 795.11 ~~~~(o~, " +"4. "3 I PZ-6B 796.89 ,J 1. ,,,e "1.:55. 51 PZ-7A 780.46 28. 'Io. +5°1.4'o PZ-7B 784.46 8. 2.1.. · "t:J.C,. 20 PZ-8 767.99 1.?,C) 7lo<:>. I.'/ PZ-9 788.96 ~2.<1 I.,. +-s<c.. 0-0 PZ-10 784.65 3q . --=11--1-4</. 86 PZ-11 805.48 .5"'.!. 'Z,) 75' ;2 .15 PZ-12 749.41 0-1:l\J t' '-/"I. 4: I PZ-13 776.51 Zt.33 -..-:;_ I 8 OT-lR 771.44 ;n.1c 7'f'-/. 3'-f -,z.z. '5S" ~_!c-1. . .!.!~:~~ 51.00 7£:3.o t . •..l" OT-3 792.88 1:s.31--=,-z:;-.s1 I I I I I I I I I I I I I I I I I I I Date: 11 :rv...'---1-=t1.. Hoechst Celanese -Shelby, NC Water Level Measurements Page:..A... of ...A Measured by: 1,M'~ • ML-~ • Measurement Device: Electronic Water Level Indicator Monitoring Measuring Depth to Water Level Comments Location Point Water Elevation Elevation (ft) (ft,msl) (ft/msl) OT-4 790.28 5:2.1-'i --::f~~-4'5' OT-5 784.00 ·5q_ 7.2-+ 4<j • -:i--e, OT-6 787.4S (a.o~ -=1J-=!.4'5 OT-6A 798.68 '1-I. e.s-"1-2(,,. 83 OT-7 782.16 al -(., -=l--'tsa. 49 OT-7A 782.S2 9.99. "1-~2 . .,, OT-8 782.26 ::n-. o"'--:i-s 4. 81 OT-10 804.08 ).$ ,l,l.i, -=l?-9-i 71 IT-1 814.20 "2,c.'10 "'.f'R "3. 3 0 IT-2 813.85 ?'.1.. 't'.::,--:J 9--n 9 Cl IT-3 809.66 ~-"?--0 -::; P,\), 41~ IT-4 809.08 'J..\.~£5 G., -L, .,,~. Js• 784.'./3 ,., ~1 IT-5 810.64 .,,,_ 'l '1 +1-B. 8+ IT-6 812.20 11--". 'b ')..._ ".?-SJ.. ~8 IT-7 813.S2 :)<\.?-S J~r-,~ ?' t% , Bio. ;z::t IT-SR 813.04 '3'2. '2. '2. --:i I:, C) • S2 IT-9 808.73 2Lt.'\1--=18s. +Co PEW-1 846.85 s:R.C?D ~sr-.'9'5 PEW-2 848.92 55-"10 -...,..,.,,.r,t~'-1C,,c:::,, • ~ '1,t..l'" ... ..., PEW-3 849.25 4-l.. ~9 \'oO"l..'e "'° PEW-4 848.14 41-W-t 80:>. <., -::i.,. ·-- - - - - - - - - - - - - - - - - - Monitoring Location AA-54 CC-33 EE-58 FF-34 FF-62 GG-61 llll-48 llll-77 K-28 P-58 T-35 V-23 C-49 OTCI ITCI OTEF ITEF Measured by: MPO. MLK Hoechst Celanese-Shelby, NC Water Level Measurements Page: I Of I Measurement Device: Electronic Water Level Indicator Date Measuring Depth to Water Temperature pH Specific Comments Point Water Level (OC) (SU) Conductivity Elevation (ft) Elevation (umhoslcm) (ft, msl) (ft, msl) 07112196 782.16 33.66 748.50 25.0 5.00 275 07/12196 812.68 22.34 790.34 17.5 6.45 350 07112196 794.48 23.20 771.28 19.0 6.31 79.1 07112196 772.73 12.85 759.88 15.2 9.25 68.0 well dry at 6.00 gallons 07/12196 772.19 14.45 757.74 15.5 6.83 79.4 well dry at 12.0 gallons 07/12196 771.78 20.47 751.31 15.3 6.64 116 07112196 755.44 37.65 717.79 19.0 5.96 50.8 well dry at 4. 00 gallons 07112196 755.87 38.25 717.62 18.0 6.57 86.6 07/11196 811.20 16.78 794.42 25.0 6.42 150 07/11196 788.12 22.49 765.f}a, .. 25.0 6.82 440 07/12196 777.38 13.65 763,!13 "" 19.0 5.66 565 well dry at 7. 62 gallons 07/11/96 811.89 14.09 1 797.80 17.8 5.13 5770 07/12196 864.11 15.47 IA" --lYT_?,• :=: . -~ '8' 18.0 5.50 23.1 07/12196 NIA NIA NIA 19.0 6.11 497 07112196 NIA NIA NIA 23.0 5.31 1770 07/12196 NIA NIA NIA 21.0 8.48 422 07/12196 NIA NIA NIA 25.0 8.22 3500 -------------------Field Data Information Sheet For Groundwater Sampling Page J_ of?.,\ Date (MM-DD-YY) ., I l"J-\9(,., Field Personnel MPQ,MLK Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID# T-'>~ Weather Conditions c.(0.J0'1 ~r'()'( Air Temperature oc. Total Well Depth (TWO) = ' 3'7.0 Depth To Groundwater (DGW) = l 3_ 1,)- Length Of Water Column (LWC) = ~', 35°" I Casing Volume (OCV) = LWC x o.11.1i = o-il gal. 3 Casing Volumes = 11. i--13 gal. = Standard Evacuation Volume Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuanon and CoUecrmo Methods TB -Teflon Bailer SSB -S1.ainless Steel Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) '7.\Q ).._ gal. TB SSBt wW .JGP Other TB SSB ('WW _AP Other Constanls for Casmg Diameters u· = o.092 s· = 1.02 2" = 0.163 6" = 1.47 3" = 0.367 7" = 2.00 4" = 0.652 8" = 2.61 ,ttl < 1/~l1t. FIELD ANALYSES 0 =3-~~ l z I '7.{.. d--- I l: 2.s-\ ''. '.:)() I : "-1,p 5.7g c;-'11 c;.!o~ 'd--0 . 0 \°t, 0 l~-o Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 _.-...., Casing Diamet;s,. --z . o inches Casing Material: PVC(:_ Metal -Guard Pipe:( PVC) Metal -No Locking Cap: <_y...,e N -~ Protective Abutment: y <...w Integrity Satisfactory: (Y-N -Well Yiel°{ Lo~ -Mod. -High R,macks: - -"'2.---1 PiT ,_c..,-..... WELL SAMPLE TIME: I I .' -ID - SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* s-oo c;oo ~()r\ -5~5 - 0 D 0 ODOR (SUBJECTIVE)•• • I • CLEAR 2 • SLIGI IT 3 • MODE RA TE 4 • IIIGII 0 0 n .. I• NONE 2 • FAINT 3 • MODERATE 4 • Sl llONG ..., - - - - - - --· -~ - --- - - - - -Field Data Information Sheet For Groundwater Sampling Page 2.,_ of '2../ Date (MM-DD-YY) If Jv \"' I "( "l(o Field Personnel MPQ, MLK Casing Diameter: Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 2. (.) inches Casing Material: Q:YP-Metal Guard Pipe: PVC (Meta!) No Locking Cap: ( Y -l N - Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Protective A~nt: (_ Y_) N Integrity Satisfactory: C,_} N Well ID# lZ-'2. 8 Well Yield[Law jMod. -High Weather Conditions C lvv,'.l'f Air Temperature oc. Remarks· Total Well Depth (TWD) = z_ 'b. oc. Depth To Groundwater (DGW) = 1l :1g Length Of Water Column (LWC) = II. d-'}... 1 Casing Volume (OCV) = LWC x o.,~3 = /.& > gal. 3 Casing Volumes = c;. '-Ii gal. = Standard Evacuation Volume Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuanon ;md CoHecnoo Methods TB -Teflon Bailer SSB . S~inless Steel Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) ,;. 1-\C/ - TB SSB ~ GP Other TB SSB ~ GP Ocher Constanrs for Casmi: Dmmerers 1.5" = 0.092 2" = 0.163 3" = 0.367 4" = 0.652 0 /(~·. &fo (.,;_ O(o is.o '1<: D 0 5" = 1.02 6" = 1.47 7" = 2.00 g• = 2.61 I. :3 3 /6:...(') I..,.) s 2.:;-:o h,-o D 0 gal. FIELD ANALYSES $.lo6 5"-'-11 Ii,, s-o /(,: ;j-,,,-- G-3~ (_,,<-.\;?- ~s-.o 2c:;-_ o ,c-u 1c,~ 0 0 u 0 '=7 /50 -TURBIDITY (SUBJECTIVE)* ODOR (SUBJECTIVE)•• • I = CLEAR 2 = SLIGIIT 3 =MODERATE 4 = IIIGII .. -I -NONE 2-FAINT 3-MODERATE 4 -SI RONG WELL SAiPLE TIME: f ,.:;re Bcmark:r -------------------Field Data Information Sheet For Groundwater Sampling Page.1._of"J../ Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 - Date (MM-DD-YY) '71,tl'lto Casing Diameter: :;i .o~ches Casing Material: / PVO -Metal Field Personnel MPQ,MLK Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID /I ~ Weather Conditions Total Well Depth (TWO) = Depth To Groundwater (DGW) = Length Of Water Column (LWC) = I Casing Volume (OCV) = LWC x 3 Casing Volumes = Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuanon and CoHccuon Methods TB -Teflon Bailer SSB -StainJess Steel Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) 1 ...,yt ~ p. ·:,"Z c.,[_,_,D't Air Temperature oc. <:" 'l .-.\0 d"J... '-{,. ~ "','l I C),( I.] = 5.e~-gal. ('l.'.:>> gal. = Standard Evacuation Volume Cf.a.\_ gal. TB SSB ( . VUI.I GP Other -= TB SSB ('v_Y GP Other Constants for Casmg Diameters 1.5" = 0.092 5" = 1.02 2· = 0.163 6" = 1.47 3• = 0.367 7" = 2.00 4• = 0.652 g• = 2.61 FIELD ANALYSES 0 s--. g <;-" I f/P/'7 I I• -I j'l :I 0 I rJ; IJ It?: 2-;- (,_ "'((p l _vt?> lR-3?--.. ?-.c;,o 'J...c;.D ~").O Guard Pipe: PVC?-Metal) N_o Locking Cap: (5_)-N Protective Ab';!!._ment: vu Integrity Satisfactory:~- Well Yield:(_Lo~ -Mod. -High Rtrnarks· -----WELL SAMPLE TIME: I • ~ i'l:'l..7 Remarks· 11n '( ,..., 7.00 GI <-; <IA 5ll~ 1'""1>~5- SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)• 1....I S-o 1--\ '.:)0 '-f'fo = l=.?4i+D ?-c}--"J-.. 0 C) 0 --... ODOR (SUBJECTIVE)•• • I =CLEAR 2=SLIG!IT 3=MODERATE 4=1llGH .. !=NONE 2-FAINT )-MODERATE 4-SIRONG N -------~-----------Field Data lnCormation Sheet Foe Groundwater Sampling Page-1:._of .2( Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 ~ Date (MM-DD-YY) '7k;i.l<;, -Casing Diameter: ')..;;, inches Casing Materia~VC ~etal/ Field Personnel MPQ,MLK Guard Pipe: PVC ~•Ji d -No ·~ Locking Cap:----c::t7-N ,.,-:-,. Facility Name KUBAL -FURR 1 HOECHST CELANESE, SHELBY Protective Abutment:(_V.:.._N Integrity Satisfactory: (_Y_) Well ID# c....-1.,\ '1 Well Yield: Low -Mod(: Hig'9 Weather Conditions i..1.-,,.-,i Air Temperature oc. Bcma[ks· Total Well Depth (TW D) = <;'"O.D Depth To Groundwater (DGW) = 15-"\'/ Length Of Water Column (LWC) = 1'-J.):, 1 Casing Volume (OCV) = LWC x t"l. I 1.,·,, = S-· c,3 gal. 3 Casing Volumes = I iu .3 "f gal. = Standard Evacuation Volume Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuatmn and CoHecrmn Methcxls TB -Teflon Bailer SSB -Stainless Steel Bailer WW -WC!U Wizard GP -Gr~mfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* //, ,o q A";'; TB SSB ~GP Other TB SSB I GP Other Constanrs for Casmg D1amerers 1.5" = 0.092 5" = 1.02 2· = 0.163 6" = 1.47 3" = 0.3~7 7" = 2.00 4" = 0.652 8" = 2.61 ("\ :;. (., s 18-:0,'") \~',b S if.cr<o ~.'lo lqo I i>.o :)...'5. o ~-0 0 D D 0 gal. FIELD ANALYSES I \.?Jp ILP.01 l )..: l °1 1).: d-i <;". l-19 c;_~o !Ro /f,O ~-0 riJ!).0 = () 0 () () ::::.> 23. I -. ODOR (SUBJECTIVE)** • I• CLEAR 2 • SLIGIIT 3 • MODERATE 4 • IIIGH .. !•NONE 2=FAINT ]=MODERATE 4-SrRONG WELL SAMPLE TIME: ·I "l •V, Remarks· f,t.,\cl C,k ~ l ).coo N --- --- --- --Field Data Information Sheet For Groundwater Sampling Page,;--of& Date (MM-DD-YY) ll S~\-°''-' FL. i:..: Persor .... el MPQ, MLi.: Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID# v-7... s Weather Conditions Cleo, I• 1· _j._ Air Temperature oc_ Total Well Depth (TWD) = ?~-~ Depth To Groiiildwater (DGW) =--.. .. It\.()"\ Length Of Water Column (LWC) = 11.'11 I Casing Volume (OCV) = LWC x D. tl. ":> = "'.:\... ?--'7 gal. 3 Casing Volumes = i., .i I gal. = Standard Evacuation Volume Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuatmn and Colleclmn Methods TB -Teflon Bailer SSB -Srainless Steel Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) L,.-1)\ ~ gal. TB SSB W"!j/ GP Other TB SSB \Y!!f) GP Other Constants for Casmg Diameters 1.5" = 0.092 5• = 1.02 2" = 0.t63 6" = 1.47 3" = 0.367 7" = 2.00 4" = 0.652 8" = 2.61 FIELD ANALYSES t\ ')_. 1-'7 L\S~ /L:00 I l, ·-D:3 f/n'. /~- - -- - - Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 -~ Casing Diameter: "Z. • <:> __ )nches Casing Material: (PVC Neta"!'-- Guard Pipe: PVC ( MetalJ-Nu UK;Ait:ig Cap: C!)-N -.. Protective Abutment: y QI) Integrity Satisfactory: (Y__) N Well Yield: Low -Mod. -High B~marks· ... .....,,.--1\ .• nl+-,._j,;, c.'..&1'0 I A. -7 4.-'-l \ cWs\,~ ./ IC ➔ ~-"'~ . h--L\:...\..-~&.:::/ l . .:,G}}.< ~~1•r-'1.::1·-. ,o·J.o.\ -, 115.0 -4>117>-4 -= 1. '-'·\.:i. ~-,"'ZS.I 1\l....::·.J-? 1..;;ov-9'tr-:'1 ::-:: '{Vi .. 1' _.., ".1.c,<... l~_~Q..:. -7 10 1Jv.:.. ·-"> Ci-1-ib . .;-::= -:i 1./". I . 8 I WELL SAMPLE I1MJi.: 11.,;. <-;, il.: I 0-, Remarks· pH (SU) S. D).... 5-07 5-1-3 ,:;-: I '3 WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* ODOR (SUBJECTIVE)** I l"'J.l!. c;c;oo J-- '-I • I = CLEAR 2 = SL!Glff 3 ~ MODERATE 4 = lllGH l 7-"1 ~oo ).... '1 .. lfl· ~ , .,_ 't $"""°00 0 ~DOD -~:-0--77,J 2,.. '2- lf L{ I= NONE 2 ~ FAINT 3 = MODERATE 4 = STRONG - -------------------Field Data Information Sheet For Groundwater Sampling Page Jc_ of .2..L_ Date (MM-DD-YY) I J. .J' ~\"' q"' Field Personnel MPQ, MLK Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID# Weather Conditions Total Well Depth (TWD) = Depth To Groundwater (DGW) = Length Of Water Column (LWC) = I Casing Volume (OCV) = LWC x 3 Casing Volumes = Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuatmn aOO Collectmn Methods TB -Teflon Bailer SSB -Scainlcss Steel Bailer WW -Wdl Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) A f's-,;;-'-I- r l,,...,o '-c' Air Temperature oc. rel./ .rr '>:,. (.,, lo ;;u .o<4 I'.)·'"~ = 5.43, gal. t O -d--. °I gal. = Standard Evacuation Volume lo. ').°I.__ gal. TB SSB ~ GP Other TB SSB v[;l GP Other Comlan!s for Casmg Prnmeu:rs 1.5" = 0.092 5· = 1.02 2· =0.163 6"=1.47 3• = 0.367 7• = 2.00 4• = 0.652 8" = 2.61 FIELD ANALYSES 0 ~. '-f3. l. -z <.. .., .') t. r,.--3,-f '1 : 4 '-I- 5, I) .-c:.'3 ;> . 5"",0d---- Casing Diameter: 2.u Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 ._... inches Casing MateriaV. · PVC r.,etal:J ' '-- Guard Pipe: PVC-~No Locking Cap: Q'...)-N Protective Abutment~ -~ Integrity Satisfactory: Q'.)-N Well Yield: Lov(-Mod. :Jligh Rcmilrks; :-A ,,.,.l.,-Ip.~\.• M. , ,<:, c..,,_J. ... "2..- In_ 4.01 , •. \l~ ✓ 10-10-0 \ ~ -?"?,.:l /~_q,.(I', -r 'l--05 1os-.J.J -1=-10<\.'-"= ,i"/~ 1s1.,. -en. 9 1000-900 -13~• c. <,,-'t'lo ~-" -l ~--o IC 0Cl'" -8-5CC • \3\3'3'.f..(.. ~ JI.C..'J WELL SAMPLE TIME: /Q.J..9 '7 '. 'S" :}.__ '7:)"b Remarks· 5".00 WATER TEMPERATURE (°C.) 2.5".D °d--S"-0 ·zs:~ ?.. <;'.b SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* ODOR (SUBJECTIVE)** "3,-;).. 0 6 0 • I = Ct.EAR 2 = SLIGI IT 3 =MODERATE 4 = IIIGII J_qD () 0 .. "d-W :;l'l ~ _:::: t=-.275 0 0 () 0 --!=NONE 2=FAINT 3-MODERATE 4-SlllONG -------------------Field Data Information Sheet For Gcounclwatcc Samvling Page~ of2.1 Date (MM-DD-YY) '7-ns,<-o Field Personnel MPQ,MLK Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID II c..c.. -2,?:, Weather Conditions r l." ,,-..cl \.l"'-'l\_,~wj Air Temperature Total Well Depth (TWD) = . "3 ).0 Depth To Groundwater (DGW) = 2 "2.. "t.,c.f Length Of Water Column (LWC) -d ,o.1o<., I Casing Volume (OCV) = LWC x 0 .( (., 3 = I. J '( oc. gal. Casing Diame;i;r:, "2...) Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 inches Casing Material: PVC (Metal Guard Pipe{ PVC __:Ytetal -N_9--Locking Cap: ( Y -, N Protective Abutment: y l.N--Integrity Satisfactory: ( Y 1 N Well Yield: Low -Mod. (Hi]9l Remarks· 3 Casing Volumes = ')-. )-.a-gal. = Standard Evacuation Volume Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuauon and Collcctmn Methods TB -Teflon Bailer SSB -Stainless Sceel Bailer WW -Well Wizard GP -Gnmfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* ODOR (SUBJECTIVE)•• -~-'.)....~, TB SSB ~, GP Other TB SSB ~ GP Other Coosrants for Casmi: Diameters 1.5" = 0.092 2" =0.163 3" = 0.367 4" = 0.652 {) 10·. i:...g (o. IS- l"t-0 'd-0( 0 ~ }- 5" = 1.02 6" = 1.47 1" = 2.00 8" = 2.61 ,."7'1 jO::, \ lr >,t.\ ,ri·'> '2. t.-\ ') (A d-- • I = CLEAR 2 = SLIGHT 3 = MODERATE 4 = IIIGII .. gal. FIELD ANALYSES 3 . '-()' '>--2:>...._ WELL SAMPLE TIME: 10.-fv ,o,'.>'-( 1n: 3 'f Remarks· l,. )'7 . ,._[) I.,. \3,0 /'ls ;:).00 "3,00 -7 350 .., () :J d--d- I ------------~------· Field Data lnformation Sheet For Groundwater Sampl~ng Pagei2_of21 Date (MM-DD-YY) 7 / t )-l,1 c, Field Personnel MPQ,MLK Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID# I:.('.;:~~ Weather Conditions C l,.;,.,o'f' Air Temperature Total Well Depth (TWD) = llf!, ' I '; (.,l.1D Depth To Groundwater (DGW) = ?,)? ,'10 Length Of Water Column (LWC) = 'l'?, ,').... I Casing Volume (OCV) = LWC x {) ./ (:,t = .3.11~ oc. gal. 3 Casing Volumes = (/,?,4 gal. = Standard Evacuation Volume Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuauon and CoHectmn Mcihods TB -Teflon Bailer SSB -Stainless Sleet Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) i\. "' :-, i 'S".\ ').._ gal. TB SSB ,.~ GP Other TB SSB l'U/UI./ GP Other - Coostanrs for Casmg Diameters 1.5" = 0.092 5" = t.02 2" = 0.163 6" = 1.47 3" = 0.367 7" = 2.00 4" = 0.652 8" = 2.61 FIELD ANALYSES 0 3.'7] I).::;· (a q.• /lo °I: '1.U ct~30 Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 Casing Diameter: ~~nches Casing Material:_j,'VC -Metal Guard Pipe: PV<c' Metal) No Locking Cap: 7 YJ l'i._ Protective Abutment: Y/N Integrity Satisfactory:'-.XJ-N Well Yield: Low-Mod. l~ Remarks· IS-,'~ WELL SAMPLE TIME: 1cos, I/. 3'-/ 9J le--J-+ "'!v~ '\ ~ q; '<. "& C\ " I q,-f-~:y'' rr-f'1'5'f Remarks· pH (SU) rJ.fD ; __ '4'> (o.'19 ( •. > 1> CP.H WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* ODOR (SUBJECTIVE)*• f (, . I 7D 0 C> • I= CLEAR 2 = SLIGIIT 3 = MODERATE 4 = IIIGlt /IP.r- r,o 0 (j .. \ c:; '.7\ 15'.°1 , 11.0 '70 rro '70 -,_'7 11. I () (') es 0 0 t) I =NONE 2 = FAINT 3 = MODERATE 4 = SI RONG ------------~------Field Data Information Sheet For Groundwater Sampling Page~of .2l_ Date (MM-DD-YY) '71 t )_\<tlp Field Personnel MPQ,MLK Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID# r-;::: 7:,c..1 Weather Conditions C l.:...,0 '( Air Temperature oc. Total Well Depth (TWD) = 7,L/ ,<,- Depth To Groundwater (DGW) = I)...~<,- Length Of Water Column (LWC) = .2 \ ,(, :, 1 Casing Volume (OCV) = LWC x O. I/,} = 3 .S-3 gal. 3 Casing Volumes = '(:). ">"1 gal. = Standard Evacuation Volume Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuaunn and Colkctmn MelhfXIS TB -Teflon Bailer SSB -Stainless Steel Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) (h--._ Aic.~ TB SSB ~ GP TB SSB C!Jj,,) GP Constanrs for Casmg Diameicrs 1.5" = 0.092 2" = 0.163 3" = 0.367 4" = 0.652 s· = 1.02 6" = 1.47 1" = 2.00 8" = 2.61 Other Other 0 3 .s-s 01! .. 37 A: 4;)...... q_o'2. 9.)-1 1t;.'I H.to gal. FIELD ANALYSES (;,,00 ·;,, : t.1-"2 q.J..~ 1.:;-. ').._ Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 Casing Diameter: ?. 0 inches Casing Material: _yvc ~731 Guard Pipe: PVC -{Metal -)-lo Locking Cap: (_:f.)-N -Protective Ab~ent: y t.!:! Integrity Satisfactory: <...r.J-N Well Yield( Low)-Mod. -High Rcma[ks· 0fJ..'< A-T (, ,-:.Cc i - WELL SAMPLE TIME: ~ i :s-0 Remarks· SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* /,J::) 0D s-~-:::: t:?~'v.O 0 {) 0 ODOR (SUBJECTIVE)** • !=CLEAR 2=SLIGIIT )=MODERATE 4=IUGH 0 D D .. .. I= NONE 2 = FAINT 3 = MODERATE 4 = Sl RONG - - - - - - -·-... - -- --Field Pata Information Sheet For Groundwater Sa1nuling Page /u of .zj_ Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 Date (MM-DD-YY) ri I I).'"'"' Casing Diameter: 2-~-inches Casing Material: PVC (__Metal Field Personnel MPQ,MLK Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID# Ff1o;}.. Weather Conditions C {c,;o~ Air Temperature oc. Total Well Depth (TWO) = Depth To Groundwater (DGW) · = Length Of Water Column (LWC) = I Casing Volume (OCV) = LWC x 3 Casing Volumes = Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuanon and Collecrmo Methods TB -Tenon Bailer SSB -Stainless Steel Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) In -:2 .'f . ,,..,, '( ', i-{j 1-'> - 01~!;, = () g(o gal. 2~.>6 gal. = Standard Evacuation Volume I l,u ()" ~ -~ gal. TB SSB (W':i/_7 GP Other TB SSB ( WW) GP Other . Conslants for Casmg Dmmetc;rs u· = o.092 5• = 1.02 2" = 0.163 6" = 1.47 3• = 0.367 7" = 2.00 4" = 0.652 8" = 2.61 FIELD ANALYSES l) '7,(, L, ,~.o 0 :.;d-0:00 Cf': .JC-; ~.'.l.'1 "x .\ 0 I. .'b?:, l<".~ It;:,;-,c;.S-- Guard Pipe: PVC(-Metal)-No - Locking Cap:{ _V N _ Protective Ment) Y(_ t-1) Integrity Satisfactory( Y)- Well Yietd: Low _,,Mod. -High Remarks· OP---t ,,,_ T l ~.c)r..o. / ,, WELL SAMPLE TIME: C,; I<) Remarks· () a fill a. , ,.)...o., I WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* (oO 5<; (,; '5" ;: ~ t-J({'-/ 0 0 () 0 0 0 -ODOR (SUBJECTIVE)•• • I = CLEAR 2 = SLIGIIT 3 =MODERATE 4 = l!IGII .. I= NONE 2-FAINT 3 = MODERAlE 4 -STRONG N - -------------------Field Data Information Sheet For Groundwater Sampling Page jJ_ of?. I Date (MM-DD-YY) '1 I O.l<i l., Field Personnel MPQ,MLK Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID# iJ 1-l --I z. Weather Conditions ,l--L, <-J~-0'( Air Temperature oc. Total Well Depth (TWD) = '--it. 00 Depth To Groundwater (DGW) = <7,'].(o; Length Of Water Column (LWC) -. {O. ~ b. I Casing Volume (OCV) = LWC x (). ,, , = /,6'1 gal. 3 Casing Volumes = <:,or, gal. = Standard Evacuation Volume Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuatmn and Collecuon Me!hods TB -Teflon Bailer SSB -Stainless Steel Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* I-\. 0 - TB SSB \_/WW) GP Other TB SSB rt'WJ GP Other Consrams for Casmg Drnmeters 1-5" = 0.092 5" = 1.02 2" = 0.163 6" = 1.47 3" = 0_367 7• = 2.00 4"-=0.652 8"=2.61 0 {.1,,; I ).,·,..\.O p .. :~s- ( .. o't [_,, .o :>- \'1.o rq.o S-o ~) 0 0 0 0 gal. FIELD ANALYSES 3-~? i':l,)) . s-'\'")... li-O 5() 0 D Shealy Environmental Services, Inc. 1(16 Vantage Point Drive Cayce, S.C. 29033 - Casing Diameter: J--~ches Casing Material: _!'VC (Metal Guard Pipe: PVC( Meta!)~ Locking Cap: <.:!.__} N _ Protective Abutment: Y-{1:!_, Integrity Satisfactory: "(V-N --Well Yielr 'Low l Mod. -High Remarks· AJ' ~ '{ A,, i-to,( y.r..l!,l ..f .o<::> WELL SAMPLE TIME: I 3:oo Remarks· II.,·. oD e::; .9_ lo ((\11_-1 I+'> ~.o.,( \q_.o ~½ , 50.8 .-, 0 0 ODOR (SUBJECTIVE)•• • I :CLEAR 2:SUGIIT ]:MODERATE 4:IIIGII •• !:NONE 2:fAINT ]:MODERATE 4:SlRONG -------------------t-.ield Datu Information Sheet For Groundwater Samuling Pagej2:_of& Date (MM-DD-YY) e,7\1)...b_, Field Personnel MPQ,MLK Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 Casing Diameter: Q_, a... inches Casing Material: PVC {MetaV Guard Pipe: PVC (Me~-No Locking Cap: ( YJ 1b.._ Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Protective Abutment: y /. N Integrity Satisfactory( "'!)-N / V --,_, Well ID# I,\ \~ rt '1 Well Yield: Weather Conditions '! -"',) Air Temperature oc. Remarks· Total Well Depth (TWO) = 'l'l-°1 Depth To Groundwater (DGW) = ti,~_,_,;- Length Of Water Column (LWC) = "> 'l,\,,') I Casing Volume (OCV) = LWC x ().(lo? = / n l..f (,, gal. 3 Casing Volumes = \°t •?~ gal. = Standard Evacuation Volume Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuatmn and CoUectmn Methods TB -Teflon Bailer SSB -Stainless Steel Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* ODOR (SUBJECTIVE)** \4.':.J~ TB SSB ('W'j/...) GP Other TB SSB ( W"!f,I GP Other Constancs for Casmg Diameters I.S" = 0.092 2" =0.163 3" = 0.367 4• = 0.652 0 11:. ·. o,f- &-c.t~ 19-,o VJ CJ 0 5• = 1.02 6" = 1.47 7" = 2.00 g• = 2.61 &-'t' i'~·~\O lo-S-~ 1i.o . (o5' () 0 gal. FIELD ANALYSES ,~_'fJ.._ ,ci. 32? 11· i7 1--i..: "1X {.; '5" t-/ l9-5f7 /-8. 0 1-8.D r-tD 1t; - 0 0 0 0 Low -Mo<\_-High WELL SAMPLE TIME: I?.~ ~o Bcmarks; ~ 'B<o. (p • I = CLEAR 2 = SLIGHT 3 =MODERATE 4 = IIIGII .. --I= NONE 2 = FAJNT 3 -MODERATE 4 - S rRONG -------------------Field Data Information Sheet t"'or Groundwater Sampling Page /3 of 2, \ Date (MM-DD-YY) l".:1. ~'" l'l'I G Casing Diameter: -i,.o Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 -inches Casing Material: ~Metay Field Personnel MPQ,MLK Guard Pipe: PVC -t1"1~ ~ Locking Cap: {:!.-) N Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Protective Abutment: y ✓N {ntegrity Satisfactory: { Y) N -~ Well ID II GG. -1,.,1 Well Yield: Low -MO<( -HiRb-,' Weather Conditions c.l~..,.o'f Air Temperature oc. Remarks· Total Well Depth (TWD) ;;;re:;., !o ii,,-~ 7/,,J~1, G:, 1.0 Depth To Groundwater (DGW) = ,~ .... ,1,1~ t;. 'iG :lo .'-1'7 Length Of Water Column (LWC) = 'iD-~3 I Casing Volume (OCV) = LWC x /). /~ S = <.,. lo I gal. 3 Casing Volumes = I "I :Z, 3 gal. = Standard Evacuation Volume Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuanon and Collecuon Methods TB -Teflon Bailer SSB -Stain1ess Steel Bailer WW -Well Wizard GP -Gnmfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* ODOR (SUBJECTIVE)•• I ~-l> -i,. TB SSB t.:!!31 GP Other TB SSB l(WYJ GP Other Coostanrs for Casio~ D1ame1ers 1.5" = 0.092 5· = 1.02 2" = 0.163 6" = 1.47 3• = 0.367 7• = 2.00 4• = 0.652 g• = 2.61 D l, (.. / "23:03 q__ : IJ- lo-iL-J L,.£1'7 ·-i. 5. o IS". 3 ,::2.. ...\O IQQ 6 D 0 0 gal. FIELD ANALYSES I~-~;)... l'f. 8 3 "'i?·. :lb 0'6'3 .:i C.'13, /,,. to'-1 15":'?> I').; 9~ 0C.: 0 0 () 0 r llin • I =CLEAR 2=SLIGIIT ]=MODERATE 4=111GII .. l=NONE 2=FAIN1 ]=MODERATE 4=STRONG WELL SAMPLf TIME: "5i' :~ Remarks: - - - - - - - --------- - - -Field Dala Information Sheet For Groundwater Sampling Page ft of 7.l Date (MM-DD-YY) 17\11\'1(0 Field Personnel MPQ,MLK Facilily Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID# DF. I I Wealher Condi1ions c,l..,o -r' Air Temperalure Total Well Deplh (TWD) - Deplh To Groundwaler (DGW) = ?:,i!'lu Lenglh Of Waler Column (LWC) - I Casing Volume (OCV) = LWC x = oc_ gal. 3 Casing Volumes -gal. -S1andard Evacua1ion Volume Tolal Volume of Waler Removed = Melhod of Well Evacua1ion Melhod of Sample Colleclion Evacuatmn arxl C0Uec1mo Methods TB -Teflon Bailer SSB • Stainless Scecl Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* ODOR (SUBJECTIVE)•• TB SSB WW GP C TB SSB WW GP Constants for Casmg Diameters I.S" = 0.092 2· = 0.163 3" = 0.367 4" = 0.652 0 ir-J:~ -l_.11~ s· = 1.02 6° = 1.47 1· = 2.00 8° = 2.61 ;!i-'s-b,' s-- !i-<-f 40 r 0 0 gal. ' -- 01he.V ~ev' FIELD ANALYSES '-ls., Casing Diameter: Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 inches Casing Material: PVC -Metal Guard Pipe: PVC -Mela! -No Locking Cap: y -N Protective Abutmenl: y -N lntegrily Salisfactory: y -N Well Yield: Low -Mod. -High Remarks: E ){-hi..(\., .h--,..., . '_,.__lf WELL SAMPL'5 TIME: /jir::, Remarks· • I = CLEAR 2 = SLIGI IT 3 = MOD ERA TE 4 -lllGll ---.. !-NONE 2=FAINT 3-MODERAlE 4-S!RONG - - - - - ----------- - - -Field Data Information Sheet For Groundwater Sanrnling Page /.;-of "2-/ Dale (MM-DD-YY) '7 -I I -c, (, Field Personnel MPQ,MLK . Facilily Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID# Ps---i --z_ Wea1her Condi1ions c--L. "'0'-f Air Temperalure Total Well Deplh (TWD) = q(;.'& Deplh To Groundwater (DGW) = '.)J.' 0 Lenglh Of Waler Column (LWC) = 1 Casing Volume (OCV) = LWC x = oc. gal. 3 Casing Volumes = gal. = S1andard Evacua1ion Volume Tola! Volume of Water Removed = Melhod of Well Evacua1ion Melhod of Sample Colleclion Evacuauoo and CoUecuon Methods TB -Teflon Bailer SSB -Stainless Steel Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* gal. TB SSB WW GP ~1h':_i'.) TB SSB WW GP OllhPt Consrancs for Casmg D1ametcrs 1.5" = 0.092 5• = 1.02 2" = 0.163 6" = 1.47 3• = 0.367 7• = 2.00 4 • = o.652 s· = 2.61 FIELD ANALYSES 0 ('?;)-( . ,,, (,.~.,) 2.'>-a ?.S-/ ~S-o c} (') Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 Casing Diameler: inches Casing Ma1erial: PVC -Me1al Guard Pipe: PVC -Mela( -No Locking Cap: y -N Pro1ec1ive Abutment: y -N In1egri1y Sa1isfac1ory: y - N Well Yield: Low -Mod. -High Remarks· ~-\(7"jl-f0,Lt-fc..-'-v--><-l I . WELL SAfrltLE TIME: {' , ,-_s- Remarks· ODOR (SUBJECTIVE)** • I a CLEAR 2 = SLIGIIT 3 • MODERATE 4 • IIIGII .. -.. !•NONE 2=FAINT )-MODERATE 4-SIRONG - - -- - -- - - - - - - - - - - - -Field Dato Information Sheet J◄or Groundwater Sampling Page ff of '2-I Date (MM-DD-YY) '7 I I I !"le..., Field Personnel MPQ,MLK Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID# Ptw Weather Conditions ( l->..10Y Total Well Depth (TWD) = Depth To Groundwater (DGW) = Length Of Water Column (LWC) = I Casing Volume (OCV) = LWC x 3 Casing Volumes = Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection EvacuatlOn and Collc:cuon Methods TB -Teflon Bailer SSB -Stainless Steel Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* -3 Air Temperature oc. Lfl,. ,4 = gal. gal. = Standard Evacuation Volume gal. - TB SSB WW GP ( Other} TB SSB WW GP (O~ei) Constants for C.rnor Prnmctc:rs u· = o.092 5· = t.02 2" = 0. t63 6" = l.47 3" = 0.367 7" = 2.00 4" = 0.652 8" = 2.6t FIELD ANALYSES 0 /'7:'i(p (o. '.)o :) .. .5:0 t../:.S-?'-\-5.c 0 ~ Casing Diameter: Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 inches Casing Material: . PVC -Metal Guard Pipe: PVC -Metal -No Locking Cap: y -N Protective Abutment: y -N Integrity Satisfactory: y - N Well Yield: Low -Mod. -High Remarks; {;y._ 1.-'be-> . <.. u WELL SAo/¥1-:E IIME: I : .'.> i::,. Remarks· ODOR (SUBJECTIVE)•• • t = CLEAR 2 = SLIGtIT 3 = MODERATE 4 = lUGH --.. t =NONE 2 = FAINT 3 -MODERATE 4 -SlRONG --·-- - - - -- - - - - - -- -- -Field Data Information Sheet For Groundwater Samplin1: Page f1of 2-1 Date (MM-DD-YY) <1 l1,\"t\O Field Personnel MPQ, MLK Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID# pe:w '--f Weather Conditions e--L.;.-.J I.) -I Air Temperature oc. Total Well Depth (TWO) = Depth To Groundwater (DGW) = Ys-'-¼'7 Length Of Water Colunm (LWC) = I Casing Volume (OCV) = LWC x = gal. 3 Casing Volumes = gal. = Standard Evacuation Volume Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuarmn and Collecuon Methods TB -Teflon Bailer SSB -Stainless Steel Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)• gal. TB SSB WW GP Other TB SSB WW GP Other Constants for Casmg Diameters u· = o.092 s· = 1.02 2" = 0.163 6" = t.47 3• = 0.367 7• = 2.00 4• = o.6s2 s· = 2.6t FIELD ANALYSES 0 { ".''-\ '> 5. 38 ~i;-.o c;<;"" -~65'.D () J- Casing Diameter: Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 inches Casing Material: PVC -Metal Guard Pipe: PVC -Metal -No Locking Cap: y -N Protective Abutment: Y-N Integrity Satisfactory: y - N Well Yield: Low -Mod. -High Rcmacks: (: ,c:+~,.,_, ...,._,~.LI WELL S~~\E._{!!4E: Remarks; ODOR (SUBJECTIVE)** • I =CLEAR 2=SLIGIIT )=MODERATE 4=111GH .. --.. I =NONE 2=FAINT )-MODERATE 4-SfRONG -- - - - ----------- - -Field Pata Information Sheet For Groundwater Sampling Page/'/ of ::2( Dale (MM-DD-YY) ·-0-'-<1>'~~'1~ I , "' I Gr 11..J'-' Ci.\.. Field Personnel MPQ,MLK Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID# LTCI Weather Conditions Air Temperature oc. Total Well Deplh (TWD) = ~ Deplh To Groundwater (DGW) = ' y Lenglh Of Waler Column (LWC) = '\ J \ I Casing Volume (OCV) = LWC x = gal. 3 Casing Volumes = gal. = Standard Evacuation Volume Tola! Volume of Waler Removed = Melhod of Well Evacuation Melhod of Sample Collection Evacuatmo and Collectmn Methods TB -Teflon Bailer SSB -Stainless Scee! Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* ODOR (SUBJECTIVE)** TB SSB WW GP Olher TB SSB WW GP O1her Consiants for Casmg Diameters 1.5" = 0.092 2" = 0.163 3• = 0.367 4" = 0.652 0 ,'il:cl-1 . S-:1...I -:i.~.o l'7oO t) ~ s· = 1.02 6" = 1.47 7• = 2.00 s· = 2.61 ,✓/7(J;B gal. FIELD ANALYSES Casing Diameter: Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 inches Casing Material: PVC -Me1al Guard Pipe: PVC -Me1al -No Locking Cap: Y-N Pro1ec1ive Abu1men1: y -N Jntegrily Sa1isfac1ory: y -N Well Yield: Low -Mod. -High Remarks· Pr .:J--e s. s Po.~-1- WELL SAMPLE TIME: I iJ ·. "'l~- Remarks· • I= CLEAR 2 = SUGIIT 3 = MODERATE 4 = IIIGII ---.. .. I -NONE 2-FAINT )-MODERATE 4-SIRONG - ------- -- -·-- -- - - - - -Field Data Information Sheet For Groundwater Sampling Page jJ_ of 21_ Date (MM-DD-YY) tl:J.._,__C_S:c;: _Jr,.t, - t.2.::r-\.-. C\ \o Field Personnel ' MPQ, MLK Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID# ~1£P Weather. Conditions Air Temperature oc. Total Well Depth (TWD) = '\ Depth To Groundwater (DGW) = A Length Of Water Column (LWC) = \ ' I Casing Volume (OCV) = LWC x = ' gal. 3 Casing Volumes = gal. = Standard Evacuation Volume Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuanon and Collecrmo Methods TB -Teflon Bailer SSB -Stainless Steel Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)• TB SSB WW GP TB SSB WW GP Constanrs for Casmg Dtam,rers 1.5" = 0.092 2" = 0.163 3" = 0.367 4" = 0.652 (') 10: TI 5" = 1.02 6" = 1.47 1" = 2.00 8" = 2.61 '8-')..?.... ?-5-D Other Other '3)00 -= =7.3Soo J ] gal. FIELD ANALYSES Casing Diameter: Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 inches Casing Material: PVC -Metal ' Guard Pipe: PVC -Metal -No Locking Cap: y. N Protective Abutment: y . N Integrity Satisfactory: Y-N Well Yield: Low -Mod. -High B,marks: pfl<>._.e_.;, S pc,;0+ WELL SAMPLE TIME: Ir,• ,C- Rema[ks· - ODOR (SUBJECTIVE)*• • I = CLEAR 2 = SLIGIIT 3 =MODERATE 4 = lllGII .. ' .. !-NONE 2-FAINT 3-MODERATE 4-SIRONG - - -- - - - -- - - - - - - - - -Field [)ata Information Sheet Foe Groundwater Sampling Page'.20 of.2.L_ Dace (MM-DD-YY) t-.).-(,'.:.: C..', ,,s-'-7 .1 { 'J ..•. s:'""'\ c,-\.(, 0 3"-'-. "\'-, Field Personnel .MPQ, MLK Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID# occl Weather Conditions Air Temperature oc. Total Well Depth (TWO) = Depth To Groundwater (DGW) = I-\ Length Of Waler Column (LWC) = '\ I Casing Volume (OCV) = LWC x = gal. 3 Casing Volumes -gal. -Standard Evacuation Volume Total Volume of Water Removed = Method of Well Evacuacion Method of Sample Collection Evacua1wn and Collecuon Methods TB -Teflon Bailer SSB -Stainless Steel Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* ODOR (SUBJECTIVE)•• gal. TB SSB WW GP Other TB SSB WW GP Other Constants for Casmg Diameters 1.5" = 0.092 5" = 1.02 2" = 0.163 6" = 1.47 3" = 0.367 7" = 2.()() 4" = 0.652 8" = 2.61 FIELD ANALYSES r\ 1(:00 l,. ,r . f1.0 I fnJ 'I 1zJ.Jq1, LfL-fo = ~;,~/.-, 111- 0 I Casing Diamecer: Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 inches Casing Malerial: PVC -Mela( Guard Pipe: PVC -Mecal -No Locking Cap: y -N Protective Abutmenl: Y-N Integrity Satisfactory: y -N Well Yield: Low -Mod. -High Remarks· nru_ es_s p,._,,,_,+ I I WELL StrPyfb TIME: Remarks· I -• I= CLEAR 2 = SLIGIIT 3 = MODERATE 4-HIGII .. I -NONE 2-FAINT 3-MODERATE 4-STIWNG - - - - -------- - - - - - - - -Field Data Information Sheet For Groundwater Sampling Page2{_of 2..L Date (MM-DD-YY) "-"C-t~ 01--\\·-:s,: _, 12.,~',9" Field Personnel MPQ, MLK Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID# 0T£,f Weather Conditions Air Temperature oc. Total Well Depth (TWD) = (\ Depth To Groundwater (DGW) = \,., Length Of Water Column (LWC) = \ ' I Casing Volume (OCV) = LWC x ,., \ gal. 3 Casing Volumes = gal. = Standard Evacuation Volume Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuanoo and CoUecUon Melhods TB -Teflon Bailer SSB -Stainless Steel Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* ODOR (SUBJECTIVE)** TB SSB WW GP TB SSB WW GP Cons1ants for Casmg Diameters u· = o.092 2" = 0.163 3" = 0.367 4" = 0.652 (D r r ·ou 5?.'13 'd-1-i) 5" = 1.02 6" = 1.47 7" = 2.00 8" = 2.61 Other Other 1...C/O --:;;,-4), d-.. () &- gal. FIELD ANALYSES Casing Diameter: Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 inches Casing Material: PVC -Metal Guard Pipe: PVC -Metal -No Locking Cap: Y-N Protective Abutment: y -N Integrity Satisfactory: y - N Well Yield: Low -Mod. -High Remarks· 0\~f' ,fl{'c;:,_c.S· S Poi f-' t-. • WELL SfiMPL}1IME: /: Q Remarks; • I • CLEAR 2 • SLIGIIT 3 • MOD ERA TE 4 • IIIGH --.. .. I• NONE 2 • FAINT 3 -MODERATE 4-SlRONG CHAIN OF CUSTODY # -~r1~ 1::.wfiJ~ ,AZ Yc~fels, ""-'· - 106.Vanfage:Pointe Drive I " Cayce, South Carolina 29033 Telephone No. (803) 791-9700 Fax No. (803) 791-9111. -------·,-\; P,ge __ of __ NPDES # _____________ _ County _____________ _ CHAIN OF CUSTODY RECORD Rec.eiving Stream __________ _ Reporting Address _____________ _ SAMPLE ANALYSIS REQUIRED Outfall No. ____________ _ ,; J,~_f /,_ r-J C C, r F ,, +-PRESERVATION (CODE) LAB USE ONLY y ' i-i"'\, •. 1 ... -·o CODE: A= None Program Area (Circle) Attention u !--t., '-in ,, J I B = HNO3 ow CWA/NPDES 1 "' ~ N ;,-C =H2S04 • f & Q "' ,, 1 ~ RCRA · ,.SP/SOL Telephone No. P.O. No. • ~ "' "' ~-¥ ~ & D = NaOH · S~iLIO ·Other· s ' ~ "' E·= ICE 1 ~ u ' ' X l~ "' C ' ~ "" -C "' 0 ' ' • F = 1-\ t. .. Y,. 1'14 t, 0 0 ·~ J i-! ,. ' '-' J 0 ~ ro 0 0 !-;o ® X ·r j ~ • • ,, ,. '. Sample_ ID (Location) TIME J ~ , < 15 0 ~ 0 • ~i SESI DATE w al 0 ~ ci 0 :1! w ~~ z £ ~ ; ,, "' REMARKS ~ 0 " ·-Q ro , ro 0 ~ O) .:) LAB 1.0. Star1 l 11:t' ... I 7 H,,lS I 9'2&7/ F1msh lj ' V-23 , ✓ Start 11:r..,h l\cS 1 ) I<-2b Finish ). L\ J I -q2&72-.. Start ) .-- ·f- I rJ., l, 1,t1 3 I qz&73 ,~ '·· Fm1sh • / Start \ I\( \\., J ~. 1,, f ;,,.,,-,I 0•·7i• -"'.' C/J&7L/ .. II :r;, \-, \1~ ;' L/ l ? .P(vJ-Finish ,. ,; ., ✓ c__ ' ,. Start ) / y .. ' 11J:t, ll5G / ,o \1.. \ c., ', ' 92&7-S-PE vJ -3 Finish , ) ~ \ ✓ \ p , I Start 1 I" µ _, ·; / i 11 Jv l1 ns·5 )' 6 I!" ·; ) 92G7& Pt w 'I -' ~ " I " Finish --· I). .J j --I -~ ' -' Start '~ ,I 'V' ?I 1,/J) . ( i, / -pEw I 11T .... l .... 1:aw .. !/ C/ Zu77 ~ ~ Finish ) / ./ . fh:Jn,,, J. Start 1' ••• I, /If,-l·1 l\:;20 ' I ) I q20 78 ~ ~ i::~clq>,iiu,7 '~1.; ~ ; / Finish ~ J I J / ,, < /(i,,,/1. C>n1li/\\% ' • ~ SAMPLER -. . . Date/Time Received by (Sig.) Date/Time Hazards Associated with Sample ; Custody Seal lnlact (Clrde) iJ M\LTOf.l C+JVA I I U·f',~\J""-YES NO NONE ~ 4m•mtp. ;t\hlJ · Aecept TAC mgl1 ~ lh W ~ : Signature: • · I ?J., ,-, 9(,, 1 :i t::Rl :SQ..(J.,_,I,. ( "! A,·u V, \) 7,,-,.,'~1..;;, lli,)'✓ Recept pH '" Relinquished by (Sig.) Date/Time Received by (Sig.) Date/Time ASC.:pt Terrp. .. I I -c ._'.iinquished by (Si9/Jv 1 -1§ 1'tib?J :J u Lab _!:teceipt by (~ig.) Date/Time Received on Ice (Clrde) ·. u:_l<....v(! .. "( CZ. -. t •. ~_,i;. __ .~•(._LL l ;_ (. V ·;._".__ 7-;sq(p I Di33c) ' YES NO ICE PACK ~ _, -•• r:, ___ ... n,..,1, r,.,' CHAIN OF CUSTODY # Clie~t Name \-Iv, c. bi I C, \~, ""' • R eportmg Add ress .. 51,,J I,) we.. Attention K. q.,, ,., I=",,. \._ Telephone No. Y,. __ Sample ID (Location) DATE Start \),:J_.,, AA-5'-t Finish Start \;).J~') AP..-s~G-> Finish Start Id-J. \,.,_1 (;:,G-l,I Finish Start 12J. ,., F~-3l\-Finish Start I ;i :r ... \.J (F. \o :2 F,n1sh Start l):r. ,., Ec-5'2, Fm1sh Start 1;2 :r' I.,_'\ I TC.. \ Finish Start [,?.J, ,.., \TeF Finish ~MFLER 1 I ·c" ()vc. -\1 \,,IJ.,,_ · _zy~mt? . -\iMJ ~ -...... IJ_, __ Signature: . · Relinquished by (Sig.) . Reli"'eted by·(k . C' ) , ,U.,{--t.-v- - - 111111!:;H.,.._ E_O,..,_ ,AL &bnflel:s, •· - 106;Vantage·:·pointe Drive Cayce, South Carolina 29033 --------,J z_-...: Pago __ of __ I NPDES # _____________ _ Telephone No. (803) 791-9700 Fax No. (803) 791-9111 County ______________ _ CHAIN OF CUSTODY RECORD Receiving Stream ___________ _ SAMPLE ANALYSIS REQUIRED 0 tfall No u C, '( A <-PRESERVATION (CODE) LAB USE ONLY = CODE: A= None Program Area (Circle) ,o -B = HN03 " "' ' DW CWA/NPDES ,,. 2 cl " C = H2S04 " 2 ::.c " l i RCRA SPISOL i ~ 0 P.O. No. 0 00 z-¥ i ·-D = NaOH SP/LIO Other: g 00 ' ~ 00 \.'. ·~ u ' X i] 00 ' E ·= 1fiE i -- C 00 0 <3 ' • ' ~ F = I ' 0 8 0 i~ J ® ~~ .~ -~ J g m u 0 < :;s ~ ~ ' g TIME J , < 0 ,. ~ 8• ~ ~i SESI w 0 0 ~ ;' 0 w :0 0 z s ., REMARKS ~ 00 u " . 0 m Z• , ,, m u ~ "" LAB LO. u:15,'l ) 92079 '. ) ✓ ' ~ OT)? I \ ✓ 92&714 .. O'G~ \ ,, C/2030 , -; ✓ O~)U ~ Cf 2ff8! ) ' ,. ·11 ' . 091(l ~ C/2&8l , ~ ~ V I 01) '-' 1 q2083 ~ ; _/ 10s,; 1 ' C/lt64 ~ le, ✓ ✓ ✓ , YZ&85 ,~ss !_; ' y. l J ✓ Oate/Tiine Received by (Sig.) Oate/fime Hazards Associated with Sample Custody Seal Intact (Clrcle) YES NO NONE Receipt TRC mo' Ar~ .... j Ju \,9'-o l'"f()\) < \ ). -':)-:.., \.-~·\.. 1"{0v ' c.;_)(l<,_,u1•l Recef)tpH '" Date/TilTle Received by (Sig.) Date/Time I I Recept T~~--c Date/Time Lab Receipt by (Sig.) ') Date/Time ~ecelved on Ice (Circle) ?15 q1, I 6QJ0 ( ; I l ( \t. . ,_ 'ISlfCQ I 08),() YES NO ICE PACK --~-'~' ; --CHAIN OF CUSTODY # ' ;:5\,,,J \,, \.J\.. \\c, \-l r';) •·· ·-\ h.-Attention Telephone No. P.O. No. Yr. \·~1'->\_.i J g ~ a, · Sample ID (Location) TIME J ~ ~ DATE w 0 0 ;: "' " <!) Start ;:; I, J, I~ II 0'5 ·oTC I Finish ' Start \.).T...,\, IJIQ qTE-r Finish ,. Start \-;;lS., \) 114 \:l ;T,-3S Finish y p( ,e_ , •• .1<.'-. Start ..) 1::3~,-, 12 Qi) ~~,~:!: -·\ Finish . --->< Start 1~::r.t-1..., 1225 (> '-t 9 Finish < Start \J..3,., .. , f'5C" Hl-\-4~ Finish X Start ,. . \J.Jv\..') 13,,;, HH-,1~ Finish X Start : 1(, e IS\,,-\< .. 10:r .... 1...") Finish llllbn~ c-v1,IJlb. ,Al!!'!lcrl-;:,, "'8. • ~ " 8 0 • 7, ) > 4 ) ; 3 106,Vantagell'ointe Drive Cayce, South Carolina 29033 Telephone No. (803) 791-9700 Fax No. (803) 791-9111 CHAIN OF CUSTODY RECORD SAMPLE ANALYSIS REQUIRED C t ,, ' " j -~ ~ ~ ,,, ,,. ·., l ~ 0 't ,,. ,, ~ .• "' i ~ 0 --"' • ,,. "' ·-u • X ~~ "' " • 5 i~ "' ~-. • t -J ~E -~ E " a ~ X ~ ~ ~& -~ "~ r g w ~I "" ' --,' 0 w r z 0 0 0 m '" ~ m m "" " 1,,, r -~ "j v J , i I 1 1- ✓ I v , 1 I l I J / ) I - - - • ___ _; -.. ,.allc/ Page _::::_of __ NPDES # _________ .c_ ___ _ County ______________ _ Receiving Stream ___________ _ Outfall No. _____________ _ +-PRESERVATION (CODE) CODE: Ao None B = HNO3 C = H2S04 D = NaOH E·=ICE F= HCI REMARKS LAB USE ONLY Program Area (Circle) DW CWA/NPDES AGRA SP/SOL SP/LIO Other· __ SESI LAB I.D. 9lfo87 9261/3 ~ 1--S-A_M_P_L_Ef!_.:._~-. --'-J_-~-.,L--D-'-a-te-'-rr"';_1_m_e_1_· -'---'rcRLe-ce-'-i-ve_dLb:cy~(S,-JigL),-L--'-'---"---'--'---'-,'---L-:D:--a-:-te";/T;:;i~mLe-'---',----,H::az-ar-,d-, -;:A_ss_o-,ci-,at-,ed-;:w-,i:::,h-:S;:a::m::p;:le---'',-;:c::c,,:::,00::,:::s;:,:::,,:::,,:::,,:::e1::1c"'1,:::ci:::,1--J ~ 11\ll-T\lN 9,VATTI.El~AVIV YES NO NONE. " f'{i~t !'lame;[) .W:.S t, · ~ -u.J .. b, .... , 'r-,.J.J\jl..JJJ-. ~ Signature: . ·. ·r23_,./,\1 11W S1L.'-..1..(·q f-c,,... t~J~\/'· 17,_:v •1----~------------J'=::...J'---'----'--f-----=---------t---'-::--:--'=----j ~ Rel!iiquished by (Sig.) Date/Time Received by (Sig.) Date/Time i: I I ~ l--::HR=•l"'·"i~-u"'is-;:h-,ed-;-:-b-y-;;(S"'ig-,.-:-,) 11 ____ ---+---::D:::a;:te";/T;:;im=e--+:cla::b-;R:-e-ce-:,-:p,::b-y::(S:-,g:-)-;--~------i----;:;D::;at;:e~/T;:::im=e--1 (""s1/JC/,-Uv n,y_C,.c, '/-1,1& I C8du -',.. ,\ r. , , c ,-~ --'7rY'f& I D311) Receipt TAC ____ ,mg,1 Receipt TefTl). ____ ·c Received on Ice (Circle) YES NO !CE PACK Pink Coov. Reoort - - CHAIN OF CUSTODY #. Reporting Address _______________ _ Telephon~ No. P.O. No. · '.:~1 Sariiple ID (Location) ~ . . . Q J Q a, TIME J ::; ~ ~ w g 0 ~ u " \...:. "-1. .j Finish f Stan Finish Start Start Finish Start Finish Start Finish Start Finish Stan < •' ~nllllll ciai_N!!.£.. 1:Alllt:H~:S, -- • .s s 5 0 0 . 3 106 ,Vantage 'Pointe Drive Cayce, South c·a,olina 29033 Telephone No. (803) 791-9700 Fax No. (803) 791-9111 CHAIN OF CUSTODY RECORD SAMPLE ANALYSIS REQUIRED i' ' { ~ ·' t ~ .. " ~ ' -~ ~¥ ~ ~ 1 i "' ~ ~ "' ' ~ ~ Q "' ] ' ' 1l lf ~ • "' ~ ' "' 0 • ' • ,~ J § • ~ " • u ' " ~ X ,B ~ c ix .!l " Q s~ w ~i ~ ~ 0 J ~ iii ~ • 0 z ~ Q 20 ~ ~ a, • r a, u~ ~ , - - ---~--· , P,ge __ of_J_ NPDES # _____________ _ County ______________ _ Receiving Stream ____________ _ Outfall No. ----c----------- +-PRESERVATION (CODE) CODE: A= Nona LAB USE ONLY Program Area (CircieT B = HN03 C =H2S04 D = NaOH ~='~1~\ · REMARKS OW CWA/NPDES RCRA SP/SOL SP/l10 Other· __ SESI LAB 1.D. • f-~-'-------'---'----~'---''-'-'-'-'--'r-'--'--'---'--''-~~~-'--'--'--'-,-'---'--'~-'=~~--'-,------,--,--,--,-,-.,:----:----'-7.--:--c--:--c:--,-:-:-:--:---1 ~ SAMPLER ; . Date/rime Received by (Sig.) Date/Time Hazards Associated with Sample Custody Seal Intact (CircteJ 8 MIL1\)N QVP.i"ll..CRf,...i,.,._,.' YES NO NONE t 14'~~~~-W-~► Signature: ·1-,rr. , q-, I,. < ) , ,-, , \_ ~ • , . ..._·,:.::. t.::!f'.,.\.)' f'_)U ~<..l.....i.._.;(<-:' '71-~" ~ -.., ~ r---, •1-,,--------,,.,---,----,--'----+-=:..:...-,,._'='--'---+-:---=':--==:,-=-:'---'----------t-~--:::-:--';;::c-----j ~ Relinquished by (Sig.) Date/fime Received b,i (Sig.) Date/Time I ' I I ~ Date/fime m61& I Off+ rl Lab Receipt by (Sig,:) : .-:._J~-·!... .. ~-"~'-A,1 ~z ( Date/Time '7 ·IJ Cfc, I D8! o White Coov: Samoler Yellow Coov. Sheatv RecePI TRC0-____ mg1 Received on Ice (Clrde) YES NO ICE PACK Pink Coov. Reoort I I I I I I I I I I I I I I I I I I I DAT A ASSESSMENT CHECKLIST REPORT . LEVEL II Client ID: Hoechst-Celanese/Shelby Prepared by: RSQ Sample Delivery Group (SDG) Description: Project Number: Date: TF026TS05 Bil.l!tfl. Ouanerly monitoring samples co)lected and analyzed by Shealy enyjronrnental for analyses of volatiles, TOC and ethylene gJyco) acconling to the sampling and analysis plan dated June 96 CONTENTS LEVEL COMMENTS II Sample Results ✓ All data Class A Method Conformance Summary ✓ Satisfactory Chain(s) of Custody (COCs) ✓ Client and project contact information incomplete (no effect on data) Master Tracking List ✓ Satisfactory Case Narrative Sample Prep Standards Prep Instrument Quality Control Data Batch Quality Control Report Surrogate Recovery Report Trip/Field/Equipment Blank Report ✓ Satisfactory Field Notes/Logbook ✓ Satisfactory CLP Forms All Raw Data Electronic Deliverables ✓ Satisfactory Discussion: For the DQOs of this project (level m to be met, the data was assessed based on reported method non-conformances and the following overall project criteria: • holding times • completeness • blank contamination • transcription accuracy • report qualifiers • comparability/consistency with historical data Class A = quantitative Class B = qualitative Class C = unusable Kubal-Furr & Associates I I I I I I I I I I I I I I I I I I I DATA ASSESSMENT CHECKLIST • 8260A (SAMPLES) Client Name: Pttpilitd By: Project Number. __ --,-__ _ Date: ~196 LAB/LOCATION ID q ~3 ~--' 7" A•~ ~ ~ COMMENTS FLAG COLLECTION/HANDLING -1/H ~ ~ -rf,1----;;;-7/,~ ~ ~w ' FIELD QC (Blab md Dupo) HOLDING TIME: / / ✓ :l'ull:t = I◄ day, ✓ Soil = I◄ clays PREP/CLEAN-UP (MeOH cxtracs) INSTRUMENT QC (1cc shoct) INSTRUMENT(Method) BLKS LCS Ouqui,al if MS '1,R fails) • Lab gmcnud cxnrol limill SPIKES (MS "'<!lliredl • Lab g........t cxnrol limill DUPLICATES (MSD) • Lab --11d. -... limits QUALITATIVE • TICS • (see sheet) REPORT / ✓ ✓ / • D:tcct. Limita, fi t4 fd CIC - LAB/LOCATION ID '11~·1'1-----= u7 "q;,JJ.¾;;" q:).t>'IO •M q~"P-!>V COMMENTS FLAG COLLECTION/HANDLING 1/tJ. ~ -111, 1(~ ~v 7/l,;I ~ FIELD QC (Blmb md Dupo) 11mo ✓ Nb HOLDING TIME: / / / / :l'ull:t = 14 day, Soil = 14 day, PREP/CLEAN-UP (MeOH cxn-acs) INSTRUMENT QC (ICC shoct) INSTRUMENT(Method)BLKS LCS Ouqui,al if MS '1,R fails) • Lab gmcnud ccmb'OI limill SPIKES (MS ""luirodl • Lab gmcnud cxnrol limill DUPLICATES (MSD) • Lab genasrod lld. dovwi<D limiu QUALITATIVE • TICS / I • (see sheet) I / REPORT ii • Detect. Llmila, foomoccs,ctc.._ f),elJ rl 'buP J i./ --- I I I I I I I I I I I I I I I I I I I DAT A ASSESSMENT CHECKLIST • 8260A (SAMPLES) Client Name: Pnµ,.edBy: Project Numbc: Dale: --?/..,.9_(, __ _ LAB/LOCATION ID r, 11.i'<!Y' t/~ V Ti, ~ ,,,,_,g;.,,-COMMENTS FLAG COLLECTION/HANDLING -f/1"-----:-v ~ u~ '1/1~ 1!:¾;;v ~ ~ ~✓ FIELD QC (ll1mu me! Dap,J HOLDING TIME: / / / ./ Yu== 14clay> liszil = 14ciay, . PREP/CLEAN-UP (McOH C11JU1) INSTRUMENT QC (ICC shea) INSTRUMENT(Method) BLKS LCS (bquin,d if MS v. &ill) . Lab......--- SPIKES <MS l'O'!wedl • Lab 1mamod ..-..I limill DUPLICATES (MSD) • Lab ...,......i ad. dmalian limiu QUALITATIVE • TICS • (see sheet) REPORT ./ ✓ / / • °"""-Limiu.-.c<c.... pr,gl£<:: ------~ -~ -COMMENTS FLAG LAB/LOCATION ID ,;~.,,_ COLLECTION/HANDLING 7/1:>-.--r✓ 7/1).~✓ 7~✓ -,~v FIELD QC (Blab mc1 Dop,J HOLDING TIME: / / ✓ / ~=14day> Soil = 14day> PREP/CLEAN-UP (McOH extract) INSTRUMENT QC (sec shea) INSTRUMENT(Metbod)BLKS LCS (R"'l'Dft'd if MS '!LR fails) • Lab......--- SPIKES (MS ""'luuodJ • Lab 1mamod ..-..i limill DUPLICATES (MSD) • Lab ...,......i ad. dcvwiao limiu QUALITATIVE • TICS • (see sheet) REPORT _/ ✓ ✓ ~ I • °"""-!.imia, fOOIDOla,CIC... fiiJ I 77U A.I, -...-~· -~ I I I I I I I I I I I I I I I I I I I DAT A ASSESSMENT CHECKLIST • 8260A (SAMPLES) Client Name: PtepmedBy: ProjcctNumber:_-,-___ _ Date: __,X,.._}'\...ua.h __ _ , ; ~ f( '--:t1 q~6f.Y.:(,, 9~ LAB/LOCATION ID q_c,r,L/e, COMMENTS FLAG COLLECTION/HANDLING ~ 1/'~"' -ti~ ~- FIELD QC (lllmb md Dup,) I HOLDING TIME: ✓ ✓ / ~ l'i.all:I: = 14 day'I .:ioil = 14day, PREP/CLEAN-UP (M.OH exuact) INSTRUMENT QC (sec ahcct) INSTRUMENT(Method) BLKS LCS l)tcquiral if MS 'l>R faih) • Lab gmcnl<d COllfflli limia SPIKES (MS requmd) • Lab gmcnl<d """"" limia DUPLICATES (MSD) • Lab gmcnl<d ad. doYwian limia QUALITATIVE • TICS • (sec sheet) REPORT / ./ / / • 0.-. Limit,. (OOID0Cel.eu:... LAB/LOCATION ID '/3~ COMMENTS FLAG COLLECTION/HANDLING ~,/ FIELD QC (Biaut, mc1 Dup,l HOLDING TIME: / / / / l'i.all:I: = 14 day, Soil = 14 day'I PREP/CLEAN-UP (McOH exuact) INSTRUMENT QC c ... tbcctl INSTRUMENT(Metbod)BLKS LCS (Roquin,d if MS 'l>R faill) • Lab gmcnl<d """"" limia SPIKES (MS requmdl • Lab gmcnl<d COllfflli limia DUPLICATES (MSD) • Lab gmcnl<d ad. doYwian limia QUALITATIVE • TICS • (sec sheet) / REPORT c/ ✓ -~ • DelecL Llmill. foomocea.crc.._ Ii' l77V _.... • .(-,,&.I& -- I I I I I I I I I I I I I I I I I I I Attachment 3 QA Summary Report and Analytical Data for the October 31-November 1, 1996 Sampling Event I I I I I I I I I I I I I I I I I I I DAT A ASSESSMENT CHECKLIST REPORT -LEVEL II Client ID: Hoechst-Ceianese/Sheiby Prepared by: R,SU Sample Delivery Group (SDG) Description: Project Number: Date: TFQ26JSQ5 121296 Fourth quarter 1996 monitoring samples co)lected and anaJyzro hy Shealy Enyjronmental Laboratories for volatiles, TOC and ethylene glycol according to the sampling and analysis pjan dated June 96 CONTENTS LEVEL COMMENTS II Sample Results ✓ All data Class A Method Conformance Summary ✓ Satisfactory Chain(s) of Custody (COCs) ✓ Client and project contact information incomplete (no effect on data) Master Tracking List ✓ Satisfactory Case Narrative Sample Prep Standards Prep Instrument Quality Control Data Batch Quality Control Report Surrogate Recovery Report Trip/Field/Equipment Blank Report ✓ Methylene Chloride detected at 0.0059 mg/L (no data qualification required) Field Notes/Logbook ✓ Some pages were missing signatures and dates. Also, corrections were made with no signature/date documentation. CLP Forms All Raw Data Electronic Deliverables ✓ Satisfactory Discussion: For the DQOs of this project (level II) to be met, the data was assessed based on reported method non-conformances and the following overall project criteria: • holding times • completeness • blank contamination • transcription accuracy • report qualifiers • comparability/consistency with historical data Class A = quantitative Class B = qualitative Class C = unusable Kubal-Furr & Associates I I I I I I I I I I I •· I I I I I I I HOECHST CELANESE Shelby, NC ANALYTICAL DATA PACKAGE Fourth Quarter 1996 Data package provided by: SHEALY ENVIRONMENTAL SERVICES, INC. 106 Vantage Point Drive Overlook Business Center Cayce, SC 29033 (803)791-9700 I I I I I I I I I I I I I I I I I I I TABLE OF CONTENTS I. Master Tracking List II. Sample Results (By analytical test method) III. Method Conformance Summary IV. Field Data Summary V. Chain of Custody Records ------------------- Client Sample Identification ITCI ITEF ITEF-a K-28 V-23 Master Tracking List I-IOECHST CELANESE-Shelby Fourth Quarter 1996 SHEALY Lab Date ID Number Collected Ground-Water 98924 10/31/96 98925 10/31/96 98928 10/31/96 98923 10/31/96 98922 10/31/96 Date Received 11/01/96 11/01/96 11/01196 11/01/96 11/01 /96 I I I I SAMPLE RESULTS I I Total Organic Carbon (TOC) I Method 415.1 I I I I I I I I I I I I - - - -·-- - - - - - - - - - - - - - Client Sample I dent ilication ITCI ITEF ITEF-a K-28 V-23 Master Tracking List -TOC HOECHST CELANESE-Shelby Fourth Quarter 1996 SHEALY Lab Date Date ID Number Collected Received 98924 10/31/96 11/01/96 98925 10/31/96 11/01/96 98928 10/31/96 11/01/96 98923 10/31/96 11/01/96 98922 10/31/96 11/01/96 Analysis Date 11/15/96 l l /22/96 11/22/96 11/25/96 11/19/96 I I 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 I SC DHEC No. 32010 Client: I Attention: I SHEALY Lab No, 98924 Description: ITCI Date Received: 11/01/96 I Date Reported, 11/21/96 I Parameters INORGANICS TOC Duplicate I TOC I I I I I I I I I I I SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method 415.1 415.1 Result 1560 1600 Units mg/1 mg/1 Terms and Conditions on Reverse Side PQL LO LO (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 10/31/96 Coll. Time: 1030 QA/QC Officer V.P. Analytical Date Date CJtwRwmoe-r,,V Prepared Analyzed Anal. 11/15/96 RES 11/15/96 RES I I 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 I SC DHEC No. 32010 Client: I Attention: I SHEALY Lab No, 98925 Description: ITEF Date Received: 11/01/96 I Date Reported, 11/22/96 I Parameters INORGANICS TOC Duplicate I TOC I I I I I I I I I I I SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method 415 .1 415.l Result 116 122 Units mg/1 mg/1 Terms and Conditions on Reverse Side (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 10/31/96 Coll. Time: 1035 QA/QC Officer Q-/<,O $ON moe-o/ . l,,'/ V.P. Analytical -~M=il"--"~--- Date Date PQL Prepared Analyzed Anal. 1.0 1.0 11/22/96 JPS 11/22/96 JPS I I 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 I SC DHEC No. 32010 Client: I Attention: I SHEALY Lab No, 98928 Description: ITEF-a Date Received: 11/01/96 I Date Reported, 11/22/96 I Parameters INORGANICS TOC Duplicate I TOC I I I I I I I I I I I SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method 415.1 415.1 Result 138 136 units mg/1 mg/1 Terms and Conditions on Reverse Side (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 10/31/96 Coll. Time: 1035 QA/QC Officer V.P. Analytical Date Date PQL Prepared Analyzed Anal. 1.0 1.0 11/22/96 JPS 11/22/96 JPS I I 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 I SC DHEC No. 32010 Client: I Attention: I SHEALY Lab No, 98923 Description: K-28 Date Received: 11/01/96 I Date Reported, 11/25/96 I Parameters INORGANICS TOC Duplicate I TOC I I I I I I I I I I I SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method 415.l 415.l Result 86 86 Units -mg/1 mg/1 Terms and Conditions on Reverse Side Coll. Date: 10/31/96 Coll. Time: 1510 QA/QC Officer <;):8Q #v(noE V. P. Analytical /11 ~ Date Date Prepared Analyzed Anal. 11/25/96 JPS 11/25/96 JPS I I 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 I SC DHEC No. 32010 Client: I Attention: I SHEALY Lab No, 98922 Description: V-23 Date Received: 11/01/96 I Date Reported, 11/21/96 I Parameters INORGANICS I TOC TOC Duplicate I I I I I I I I I I I SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method 415.1 415.l Result 10800 10700 Units mg/1 mg/1 Terms and Conditions on Reverse Side PQL 1.0 1.0 (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 10/31/96 Coll. Time: 1556 QA/QC Officer V.P. Analytical Date Date Prepared Analyzed Anal. 11/19/96 JPS 11/19/96 JPS I I I I SAMPLE RESULTS I I Ethylene Glycol I Method 8015A I I I I I I I I I I I I ------------------- Client Sample Identification ITCI ITEF ITEF-a Master Tracking List -Ethylene Glycol HOECHST CELANESE-Shelby Fourth Quarter 1996 SHEALY Lab Date Date ID Number Collected Received 98924 10/31/96 11/01/96 98925 10/31/96 11/01/96 98928 10/31/96 11/01/96 Prep. Analysis Date Date 11/08/96 11/11/96 11/08/96 11 /I I /96 11/08/96 11/11/96 I I 106 VANTAGE POINT DRIVE CAYCE. SOUTH CAROLINA 29033 I SC DHEC No. 32010 Client: I At tent ion: I SHEALY Lab No, 98924 Description: ITCI Date Received: 11/01/96 I Date Reported, 11/21/96 I Parameters ethylene glycol I I I I I I I I I I I I SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result units 8015A 840 mg/1 Terms and Conditions on Reverse Side PQL (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 10/31/96 Coll. Time: 1030 g:t>o fr);r;l)E V.P. Analytical -~(Vl'----jr./'------- QA/QC Officer Date Date Prepared Analyzed Anal. 5.0 11/08/96 11/11/96 SAG I SHEALY ENVIRONMENTAL SERVICES, INC. I Scientists and Consultants 106 VANTAGE POINT DRIVE CAYCE. SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS (803) 791 ·9700 FAX (803) 791 ·9111 I SC DHEC No. 32010 Client: I Attention: I,, SHEALY Lab No, 98925 Description: ITEF Date Received: 11/01/96 I Date Reported, 11/22/96 .I Parameters ethylene glycol I I I I I I I I I I I I HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result units 8015A ND mg/1 Terms and Conditions on Reverse Side PQL NC DEHNR No. 329 Coll. Date: 10/31/96 Coll. Time: 1035 QA/QC Officer 91w/bvmo€ V.P. Analytical ---'-M-"-~---- Date Date Prepared Analyzed Anal. 5.0 11/08/96 11/11/96 SAG I I 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 ,I SC DHEC No. 32010 Client: I Attention: I. SHEALY Lab No, 98928 Description: ITEF-a Date Received: 11/01/96 I Date Reported, 11/22/96 I Parameters ethylene glycol I I I I I I I I I I SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result Units 8015A ND mg/1 Terms and Conditions on Reverse Side (803) 791 ·9700 FAX (803) 791 ·9111 NC DEHNR No. 329 Coll. Date: 10/31/96 Coll. Time: 1035 QA/QC Officer 9,/),(J--f5,fJ7f}G V. P. Analytical fV\ I Date Date POL Prepared Analyzed Anal. 5.0 11/08/96 11/11/96 SAG I I I I SAMPLE RESULTS I I TCL Volatiles , Method 8260A I I I I I I I I ·• ,1 I I I Client Sample Identification ITCI ITEF ITEF-a Master Tracking List -TCL VOCs HOECHST CELANESE-Shelby Fourth Quarter 1996 SHEALY Lab Date Date ID Number Collected Received 98924 10/31/96 11/01/96 98925 10/31/96 11/01/96 98928 10/31/96 11/01/96 Analysis Date 11/02/96 11/02/96 11/02/96 I I 106 VANTAGE POINT DRIVE SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CAYCE, SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS (803) 791-9700 FAX (803) 791-9111 ,1 I I I I I I I I SC DHEC No. 32010 Client: Attention: SHEALY Lab No: 98924 Description: ITCI Date Received: 11/01/96 Date Reported: 11/21/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene I 2-hexanone methylene chloride 4-methyl-2-pentanone I I I I styrene 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenes HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result Units PQL 8260A 0.1370 mg/1 0.0200 8260A 0.0399 mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A 0.1320 mg/1 0.0050 8260A 0.0194 mg/1 0.0050 8260A ND mg/1 0.0050 8260A 0.0127 mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND rng/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A 0.0309 mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.00~0 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND rng/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side NC DEHNR No. 329 Coll. Date: 10/31/96 Coll. Time: 1030 QA/QC Officer <;)kifpjrno£ V.P. Analytical "'pf-/ Date Date Prepared Analyzed Anal. 11/02/96 SAG I SHEALY ENVIRONMENTAL SERVICES, INC. I Scientists and Consultants 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS I SC DHEC No. 32010 I I I Client: Attention: SHEALY Lab No, 9 8 9 2 5 Description: ITEF Date Received: 11/01/96 Date Reported: 11/22/96 I, Parameters I VOLATILE ORGANICS acetone , 1 benzene bromodichloromethane I I I I I bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 2 -hexanone methylene chloride 4-methyl-2-pentanone styrene 1,1,2,2-tetrachloroethane cetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane I trichloroethene , vinyl acetate ' vinyl chloride xylenes I I I I HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result Units PQL 8260A ND mg/1 0.0200 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0_0050 8260A ND mg/1 0.0050 8260A ND mg/1 0_0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 . 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND nig/1 0_0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND rng/1 0.0100 8260A ND rng/1 0.0150 Terms and Conditions on Reverse Side QA/QC {803) 791-9700 FAX {803) 791-9111 NC DEHNR No. 329 Coll. Date: 10/31/96 Coll. Time: 1035 Officer V.P. Analytical rf!i;ritJE ('11./ Date Date Prepared Analyzed Anal. 11/02/96 SAG I I 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 I SC DHEC No. 32010 I I I I I t I .I I I I I I I I Client: Attention: SHEALY Lab No, 98928 Description: ITEF-a Date Received: 11/01/96 Date Reported: 11/22/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 2-hexanone methylene chloride 4-methyl-2-pentanone styrene 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenes SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result Units PQL 8260A ND mg/1 0.0200 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND rng/1 0.0050 8260A ND rng/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side QA/QC (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 10/31/96 Coll. Time: 1035 Officer 900 (rmvd' V.P. Analytical M~ Date Date Prepared Analyzed Anal. 11/02/96 SAG I I I 1 I I I I I I I I I I I I I I 106 VANTAGE POINT DRIVE CAYCE, SOUTH CAROLINA 29033 SC DHEC No. 32010 Client: Attention: SHEALY Lab No, 98927TB Description: Trip Blank Date Received: 11/01/96 Date Reported: 11/21/96 Parameters VOLATILE ORGANICS acetone benzene bromodichloromethane bromoform bromomethane 2-butanone carbon disulfide carbon tetrachloride chlorobenzene chloroethane chloroform chloromethane dibromochloromethane 1,1-dichloroethane 1,2-dichloroethane 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene 1,2-dichloropropane cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 2-hexanone methylene chloride 4-methyl-2-pentanone styrene 1,1,2,2-tetrachloroethane tetrachloroethene toluene 1,1,1-trichloroethane 1,1,2-trichloroethane trichloroethene vinyl acetate vinyl chloride xylenes SHEALY ENVIRONMENTAL SERVICES, INC. Scientists and Consultants CERTIFICATE OF ANALYSIS HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087 Kathryn Frank Method Result Units PQL 8260A ND mg/1 0.0200 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 o.Oo5o 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A 0.0059 mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0050 8260A ND mg/1 0.0100 8260A ND mg/1 0.0150 Terms and Conditions on Reverse Side QA/QC (803) 791-9700 FAX (803) 791-9111 NC DEHNR No. 329 Coll. Date: 10/28/96 Coll. Time: Officer Q.r/0 (91,m<Jr;- V.P. Analytical Mfr'U Date Date Prepared Analyzed Anal. 11/06/96 SAG I I I I I I I I I I I I I I I, I I I I METHOD CONFORMANCE SUMMARY I I I 1 I I ,I I I I I I I I 1, I I I I Method Conformance Summary for 4th Quarter 1996 Hoechst Celanese -Shelby Data Criteria Volatiles TOC Sample Holding Time ✓ ✓ Standards Preparation ✓ ✓ Instrument Tuning ✓ NIA Instrument Calibration ✓ ✓ Calibration Verification ✓ ✓ Degradation Check N/A N/A Interference Sample/Standard N/A N/A Blank Results ✓ ✓ Method Accuracy ✓ ✓ Method Precision ✓ ✓ Surrogate Recovery ✓ NIA PDS/SD/MSA See Note l See Note 2 TCLP Prep N/A N/A Key: ✓ = Method Criteria Met NI A = Not Applicable * = Method Criteria Not Met -see footnote(s) PDS = Post Digestion Spike SD = Serial Dilution MSA = Method of Standard Additions Signed: bid ---· I Ethylene Glvcol ✓ ✓ N/A ✓ ✓ N/A N/A ✓ ✓ ✓ NIA See Note 3 N/A I I i I I I I I I I I I I I I I I I I Note I· Volatile dilutions Shealy Lab ID Dilution Ratios 98924 1:19 Note 2· TOC dilutions Shealy Lab ID Dilution Ratios 98922 1:999 98923 1:19 98924 1:199 98925 1: 19 98928 1:19 Note 3: Ethvlene !!lvcol dilutions Shealy Lab ID Dilution Ratios 98924 1:9 Signed: fl)/~ 7 I I I I I I I I I I I I I I I I I I I ....:'-'! Hoechst Celanese -Shelby, NC Water Level Measurements Date: 31 Oc:r /'rf(. Page:_1_ of j Measured by:__,C ........ Lt .... U....__ __ _ Measurement Device: Electronic Water Level Indicator Monitoring Measuring Deptb to Water Level Comments Location Point Water Elevation Elevation (ft) (ft,msl) (ft/msO A-39 823.36 I q. OI 8D'-l 3o B-34 790.62 fl •. ?q '7 ?L/-. 2::, C-49 864.11 i 'i.30 6'1 -Bl '.:J. ··-D-27 845.50 I 1.? 5: 5:;_ 0 I ':T D-35 845.69 t"I. 73 S26."'tr D-56 845.19 19. "{( 8 2'J.'79 D-88 845.52 19. &O S:J'i.q1 F-55 849. 19 ~(). LJ 808.'J" G-50 848.48 31.s-s-Sot/ q 3 G-88 848.26 3 5'.38 'JDC/BB H-59 845.25 <-J<l,~S BoDwO H-79 846.53 4(,,. 70 7qc1g3 I-57 837.63 ZJ 37 80Lfo<C::, J-29 825.18 23.'iO 901-38, J-59 825.01 ,2 <(, </</ goo. -=s? K-28 811.20 11.~9 7q1.3 I K-58 811.39 7 /. /7 ·,qo. 2..2 M-28 806.72 J/.o? 7 7-S-.(,,'{- M-44 806.71 7 '1:l<I 77(;. 67 N-29 803.38 !S.J?.;, 7 B 7. "fl, N-53 803.82 17. qy 7B5' S'f 0-25 807.54 I~. 7S 7qo. 71 0-59 806.61 I( •. "6 7qo. 01 P-31 790.00 .Z.2. '[7 707.I!) P-58 788.12 2 J, 77 ·7 0 '-f. 3 j- I I I I I I I I I I I I I I I I I I I y Hoechst Celanese -Shelby, NC Water Level Measurements Date: --------- Measured by: _____ _ Monitoring Measuring Depth to Location Point Water Elevation (ft) (ft/msl) Q-33 783.48 23 &<;" R-17 779.31 !?. 5'3 R-42 778.81 12..30 S-50 826.02 ZS'37 T-17 777.90 / <I. (S" T-35 777.38 I </.()'g T-58 776.03 i </ .. </5' U-38 826.55 .ZS.oJ V-23 811.89 J 7. J.3 W-23 800.91 IG-74' X-32 796.96 IG,~.J Y-38 794.52 /9.f.J Y-74 794.87 I 'f.o3 Z-78 797.08 ,< .3. 6 .3 AA-41 783.68 .17.73 AA-54 782.16 31~. 71. BB-llf If 771.75 ?. 75' CC-33 812.68 Z<f.os CC-64 811.37 ,Z I. ~'t DD-58 796.10 :?(,,.07 EE-58 794.48 <fo.oo FF-23 772.33 I 6'.J.4 FF-34 772.73 -IS-: 15" FF-62 772.19 /1'1,<fO Page:....l_ of~ Measurement Device: Electronic Water Level Indicator Water Level Comments :Elevation (ft,msl) 7-5q· R3 71.P5".'7i 7tflP.5 / 90D. C,?5" IA! 1/ 700 -1~3-?:> {JV . 'J '7~33o 7vr.ora So,. 'f'7 7q4_5L-. ,SLf.r7 7fu.4-3 t7'f&,q 170/04 7 7-.i.,, '-I>-.-· '7 -c,tr • J..f.') . I 'I 4 6-. l.ft1 7r,, .:i.oo 7?b.(P; 75q_ 3~ 7(p0.03 iff4.'f9 75"7'5?/ 7o~'.:>-.S 7 '5"1.71 I I I I I I I I I I I I I I I I I I I Hoechst Celanese -Shelby, NC Water Level Measurements Date: ---------Page:_l_ of _A Measured by:. ______ _ Measurement Device: Electronic Water l,eyel Indicator Monitoring Measuring Depth to Water Level Comments Location Point Water Elevation Elevation (ft) (ft,msl) (ft/msl) GG-25 771.64 JJ.17 7'-f'3 .. 'f 7 GG-39 770.44 ,2.L..4/ 7'+'r3.as .. GG-61 771.78 ,Z,J.(,,{ 7'-f'0./ 7 HH-48 755.44 39.t~<t 71 ~-. '7"5" HH-77 755.87 <1.'i7 7/t,, Di) PZ-1 773.99 '9. ?"? 7!:i'I-.J~ PZ-2 795.81 '.')" '9. S' r. 7 'fr'l. 2 '5'" PZ-3 786.62 ------Well destroyed/Paved over between 8/9S and ll/9S PZ-4 750.07 S:73 7 '+'-t. -',Lf, PZ-SA 788.72 J'il-39 75o .3~ PZ-SB 777.59 l.7.11 7Lf Cf'.r,,s PZ-{iA 795.11 4/.'Ro 7 'JJ ~/ PZ-6B 796.89 "I?. 71.. 7 ':54/ ,.__, PZ-7A 780.46 zq.12 7-s'f 6Lf PZ-7B 784.46 ,.s.3 , 7')-q ~ PZ-8 767.99 7.35" ,1po,w PZ-9 788.96 3S'. 9'J 75,1q7. PZ-10 784.65 <I</ . .Zo 74'0,Lt...,- PZ-11 805.48 S-</(,G 75D. 'b ;;i, PZ-12 749.41 () • (!)() 7'f1.'fl PZ-13 776.51 23 .3 0 753.21 OT-IR 771.44 2 I. 95 7'-1?/ '-/Ci OT-2 774.01 .S-o.&S-7;}}3l:, OT-3 792.88 G, S: Jo 7:;J.7-w I I I I I I I I I I I I I I I I I I I Hoechst Celanese -Shelby, NC Water Level Measurements Date: --------- Measured by: _____ _ Monitoring Measuring Depth to Location Point Water Elevation (ft) (ft/msl) OT-4 790.28 </?.4.Z OT-5 784.00 S7. l'i? OT-6 787.45 5'9 6'5 OT-6A 798.68 79.of OT-7 782.16 S,t,25 OT-7A 782.52 J0.3o OT-8 782.26 7S':27 OT-10 804.08 2.r:. . (,,2 IT-1 814.20 Jo. q.1 IT-2 813.85 37. 90 IT-3 809.66 Z.<. . .zs IT-4 809.08 2.</. 93 IT-5 810.64 <3. 7o IT-6 812.20 ?11 2o IT-7 813.52 2 7 :;;,,,.,, IT-SR 813.04 17 'ii'2 IT-9 808.73 ) ?-.~.q~ PEW-1 846.85 i' /, ,., .'i' - PEW-3 849.25 39. ft' PEW-4 848.14 'i?/, 9(,, Page:....!_ of_± Measurement Device: Electronic Water Level Indicator Water Level Comments Elevation (ft,msl) 74-,. 'oio 7~~ 'o )._ 7;!_Jv;D -71q.1.vc 7.dq. q I 77:J, ,3Q 751P 1c; 777~ 7 6 -?J ,;;_ 7 775" ,q':)- 7 SJ. 1 I 7'iY-f-.f~ 7 7& .Cflf- 7'i3J OD 7P:,5"' 7:J. 7q5~J ,:._ 19'; 7')° O'oo\t---Lc..\-o..._ ·,,,._ we\\ 7<P"J-.&:, No._, ll.Je..\ \ "'<3> 'S 'oee.,,.i.... ~cl...00~ -Poq,37 70(.p.(ff I I I I I I I I I I I I I I I I I DATE: TO: ll8 WESTINGHOUSE BOL'LEV AlUI SUITE 101 CHAllLOTTE, NC l8l73 PHONE: t704) 583--0990 FAX, (704) 583-0961 c!)ec. r~) /t/tii-~ ffohi !)~ bLu.-/-a;. 0 P. 0, BOX 3164 WILSON, SC 27895-316' PIIONE (9191 l37-J84S FAX: (919) 137-lMS COMPANY/LOCATION: c:/(uh} ~ ji;;y a/1..J" -4 r-,?Jc:,____,,, . FAX NUMBER: (-8!3-t/3I-B03C/ NUMBER OF PAGES INCLUDING COVER SHEET: 0--- FROM: Ven11,·W ur,/ COMMENTS: J.rl/' l. -F- ' ( .'/2,.-/S J..1,,,-,s t'Jn ,..() I -• j --,rf d,,;-/z-cl --/--h /Y,S,~ ,n. -ti,# .t:...i. Id '1,--/r,./;; s,lu. ~ I tu/I ......, .-. · I " r':i ,,-,,.; ~ , . -/a,/111, •/ I / / ,-..,_ ' I' 1\--( '+, T 1 l -\...,- • . . I I I I I I I I I I '-- I I I I I I I ~-· I. I Hoechst Celanese -Shelby, NC Water Level Measurements Date: 3/ Oer /?f(. Page:--1._ofJ Measured by:'-. ...l,C .... Lll,L('-llH'----Measureuient Device: Electronic waw 1,eye1 Indicator Mcmltariq .MeasarlJII Depth to Water Level Comments LocatioD Polllt Water Elevation ·Elevadon (ft) {!t,msl) . (ft/ A-39 823.36 I q. _, 80'-l3!J B-34 790.62 // -;,q 'l '74 l~ C-49 864.11 ·i ?. ?o 'o '-I;,_ B / D-27 845.50 I 1. ? S° ~.2~.J~ D-35 845-69 ,'1.7? ~45',C,I D-56 845.19 IC/. '(I B z,;.'70 D-88 845..51 ,q '·O y{ :;i ti. q '1 F·!! 849_19 'itl-(,.:J 9o6.5"C.. G-SO . 848.48 3 '{.S"S-Botl.t./3 G-88 848.26 31-31 901?. BB H·S9 845.25 4<1,(.S' 9,oQ <&>O B-79 846.53 "-//-. 711 7qq g3 1-67 837.63 ?:J 37 go•-r~e:, J-29 • 825.18 ,ZJ.fO 90t.3B J-59 · 825.01 ;_ <(, <(-./ 000.57 K-28 811.20 J<;. 'K9 7q,.3/ K-58 811.39 7 I. /'7 ,qo. 2.,2 M-28 806.72 .J/.~'i 775".l,,{- M-44 806.71 1 q Y4 77r,.P.7 N-2' 803.38 ,,:.-_ 9? 7 8 7. t=;(_ N-53 803.82 /7. qf 7Q'S'_ 9'f 0-25 · 807.54 I~. 7S 7qo.71 0-59 806.61 I( .. r,A 7qc. fol P-31 790.00 z.z. f7 71P7./?,, P-58 788.1:Z 7 J, 77 7~4.3? I I I I I I I I I I '---- I I I I I ':f I I --· I I: Hoechst Celanese -Shelby, NC Water Level Measurements Date: 3\ OJ:-1C\~<.-Page:...l_ of _j Mwurement Device: Electronic Water l,eye) Indicator Measurecl by:._~C>..).__I\_._ __ _ MonitoriD& MeamiiD& Depth to Water Level Ccmmaits Location Point Water Elevation FJevation (!t) (ft,msl) (ft/~ Q-33 783.48 J.,$. r,, 7-5tf Q3 · R-17 779.31 1:1.f:<' 1/;5.'7~ R-42 778.81 /7.1,t; !UIR.5 / S-50 826-02 25"!7 @OD.lt"5" T-17 m.9/J ! '-1 C'C:-7q;/_4'J T-35 m.38 /<l.08 '71.P3.3o T-58 776.03 j </ Q<; 7vr.o9. U-38 826.j5 ZS.6>3 Sot.Lf'l V-23 811.89 J73.J' 7qu_ "'5(,., W-23 800.91 l~-74' l'O'-f.f7 X-3.2 796.96 /I'._,:; r 7&;.4-'2, Y-38 794.52 ,~.f-1 779:(e,C/ Y-74 794.87 J f()'j , 7 o /:S 4- Z-78 797.08 z J./ • .J 772i.'-K""' AA◄l 783.68 .37. 7..7 1'15",q!; AA-54 782.16 7/,., 71. 'I i.f 'J-. /Jr, BB-lf If 771.75 11, 75' ,~ ~.oo CC-33 812.68 7'1,0"3 7~-~ CC-64 811.37 21. ~? 7'Bq,3P-, DD-58 . 796.t0 -~f...07 7fR0.03 EE-58 794.48 "lo. --'11i4.'f9 FF-23 772.33 1 'i. 74 ilf1 '5{j FF-34 772.73 ... 7o7'J-fo I~ IS" FF-62 772.19 71'1,<fO 7'5'/,7q I I I I I I I I I I I I I I I I I I I Hoechst Celanese -Shelby, NC . Water Level Measurements Date: 3 \ . :w \ C\ Ca\ 1..-Page:...l... of _j · Meam.rement Device: Electronic Water Level fndicator Meamred by~ ~~ : Monltorin& Measuring Depth to Water Level . C-Ommeats 1-0Catlnn Point Water Elevation Elevation (ft) (ft,msl) (ft/aw) GG-25 771.64 21.J7 71.f~.'+ 7 GG-39 770.44 ~~-41 -i~e.og GG-61 771.78 ,l,'J.~{ ' 7~-/7 HH-48 755.44 "? 'l ,_ q 7t"i".'J--S- HH-77 1SS.lr1 '?9.P7 71(.,_0i) PZ-1 773.99 Jq_-n -, c; 'I-It, PZ-2 795.81 ~ '9. ,,. 7~.2.", PZ-3 786.62 ----Woll dauoyed/Paved ava ~ 8195 111d 11/95 PZ-4 7$0.(11 "-7? 14-½'. 41- 1'7.-SA 788.72 'J'l,39 750 _3~ PZ-SB 777.59 t. 7. 'l I 74q,r,,5 P'L-6A 79S.11 4/, 'ill"l 7 '5J ?:ii ~ 796.89 ~, 7 ~'-t.f ..... P'L-7A 780.46 7q_,~ 75"/. ~'-f PZ-7B 784.46 ,.s.3 ,7-:i-.'7 ~ n-a 767.99 7.3) ,~o.w. PZ-9 788.96 :1'S.99 75.:J. q'2_ PZ-10 784.65 </<t. Zo 14n 14--.,- PZ-11 805.48 S-<1/,.G 75D.?J~ PZ-ll 749.41 (') • e)A 7i+r.+1 PZ-13 776.51 2$30 75321 OT•lR 771.44 z I. <1.::: 71.1'1. "-4~ OT-2 774.01 s-o. c-S"' . 7J'}3(;. OT·3 792.88 t.;5".1,..; 7.;'.l7.~ I I I I I I I I I I '···· I I I I I:. I I .......... I I Hoechst Celanese -Shelby, NC Water Level Measurements Page:j_ of..! Measured by:. _ __;;~------Measurement Device: Electronic Water I..eyeJ Indicator Monitoring Measuring Depth to Water Level Comments Location Poinl Water Elevation Elevation (ft) <n,msI> ' (ft/ms!) OT◄ 790.28 't'i,4J 74,~ OT-5 784.00 S-7. (9 7:JG,. 'o '.l OT-6 787.45 59 f', '7~1<PO -OT-6A 798.68 7'/,o'( 7fq.~o OT-7 782.16 s z. 1."' 7Jq,q1 OT07A 782.52 JO. '1" 77~.aQ OT-8 782.26 7S': 27 7':J'l,.Cfq OT-10 804.08 ;.r.. ,1 __ 7 777 L/{,. lT-1 814.20 3n.t.;:J 76~.:Z.7 rr-2 813.85 37. '10 775' ,qS lT-3 809.66 ? ( .. 2'-7S3.41 lT-4 809.08 24. Q'] 7f;lf(S- lT-S 810.64 '?,3. 711 / 7r.,. qq. lT-6 812.20 .,,, j,i 7t3.;? OD IT-7 813.52 Z 7 11>,i 7P.J,. 7;)_ IT-8R 813.04 / 7. o, 7'15.d.J lT-9 808.73 ') ~"\ .a.~ "-1 B, 115 O'oo~ ........ ~o .... ·,..._ w-\\ PEW•l 846.85 p I.,,,<" 7(;'J,&:;> . . N• we,\\ V\G~ 'oeu,_ ~--::J PEW-3 !149.25 __ { 9. ~,, 'tD/1, '37 PEW-4 848.14 'i'/, 9(.,, 7Cpw.fR ------------------- Monitoring Location K-28 V-23 ITCI ITEF Measured by: CWH SWC Hoechst Celanese-Shelby, NC Water Level Measurements Page: l.fil..l Measurement Device: Electronic Water Level Indicator Date Measuring Depth to Water Temperature pH Specific Comments Point Water Level (OC) (SU) Conductivity Elevation (ft) Elevation (umhoslcm) (ft, msl) (ft, msl) 10131/96 811.20 19.89 791.31 19.3 6.44 223 10131/96 811. 89 17.33 794.S6 19.1 5.07 4S18 I 0131196 NIA NIA NIA 20.2 5.29 122 10131/96 NIA NIA NIA 21.8 8. 10 244 -------------------Field Data lnCocmation Sheet For Groundwater Sampling Page \ of U, ---- Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 Date (MM-DD-YY) ..i'I 0 C7 '1 (. Casing Diameter: z. inches Casing Material: .PV< ·\. Metal Field Personnel CWH, GAO Guard Pipe: PVC -Metal -)No Locking Cap: Q...)- Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Protective Abutment: CD-N ·1n1egri1y Satisfactory: Well ID# /( -,z_;r Weather Conditions (~/\.,'......,. Total Well Depth (TWD) = Depth To Groundwater (DGW) = Length Of Water Column (LWC) = I Casing Volume (OCV) -LWC x 3 Casing Volumes = Total Volume of Water Removed - Method of Well Evacuation Method of Sample Collection Evacuaoon and Collccnon Mcrhods TB -Teflon Bailer SSB -Stainless Steel Bailer WW -Well Wizard GP • Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) . Well Yield: Low(-Mod.) High LOA,,,..., Air Temperature oc. Remarks· ,ZY.oo l"/.(f'f ~-If C). {t.. "1 -/.32 gal. 5-") (,, gal. = Standard Evacuation Volume 3. 9t,,_ gal. TB SSB ;ww \ GP Other TB SSB \ W"!f,I GP Other Constanu for Casmg D1amcrccs u· = o.092 s· = 1.02 2· = 0.(63 6" = 1.47 3" = 0.367 7• = 2.00 4• = 0.652 8" = 2.61 FIELD ANALYSES I.$=-132 ;z .(.4 ?.9C. WELL SAMPLE TIME: I </'I/ I <f'f<; l"i<-19 ;,r.7 Remarks· N Q) - 151"0 pH (SU) fn. </ {,_ I.. So (._ Jf ,, __ 'f<{ F. $/~,..i 1Soo WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* ODOR (SUBJECTIVE)** 2o.l/ -:foo ( .3 ' I= CLEAR 2 = SLIGHT J = MODERATE 4 -IIIGH I Y-. 7 7no I 2 .. I 1. 2 ,'7.J 2.oo 200 ·-,,. ,),;;i3 I I ;:_ ,< - -I = NONE 2 -FAINT J -MODERATE 4 = STRONG N -------------------Field Data Information Sheet For Groundwater Sampling Page ?-of~ Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 Date (MM-DD-YY) ·3 I rClc, 'JC. Casing Diameter: 2 inches Casing Material: ~Metal Field Personnel CWH, GAO Guard Pipe: PVC..= Metal .,»lo Locking Cap: <:-"r -) N Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Protective Abutment: Y-(J!.. ·integrity Satisfactory: (_.YJ - Well ID# V -.ZJ Well Yield: Low E Mod.). High Weather Conditions :Sr, L I ~ .. ...,_ Air Temperature oc. Bema[k:r Total Well Depth (TWD) = . ,Zf.oo Depth To Groundwater (DGW) = I 7 .. 1J Length Of Water Column (LWC) = /o./, 7 I Casing Volume (OCV) = LWC x O. /l,3 = ,. 7"? gal. 3 Casing Volumes = " /9 gal. = Standard Evacuation Volume Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuatmn and Collecaon Methods TB -Teflon Bailer SSB -Scainlcss Steel Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* ODOR (SUBJECTIVE)•• 5': /9 TB SSB rw\ GP Other TB SSB ~GP Other Constants for Casmg n,amerecs 1.5" = 0.092 2" = 0.163 3" = 0.367 4" = 0.652 ;;.!: IS/7' .:../. 1 "i? I '7. 5· S°ODO I 4 s· = 1.02 6" = 1.47 7" = 2.00 8" = 2.61 /. 7? /",21 4. 9q /9. f{ "'loco I 4 ' I = CLEAR 2 = SLIGIIT 3 =MODERATE 4 -HIGH •• gal. FIELD ANALYSES "?_y, 5"./9 WELL SAMPLE TIME: ,~s;c,, ,s-10 J S$;<1 Remarks· s.o/ 5.Dt I 'z. 3 I q. I 4000 ~<)OO -1--7 1.../ , b-I 9i I I ,{ 4 I-NONE 2-FAINT )-MODERATE 4-STRONG N -------------------Field Data Information Sheet For Groundwater Sampling Page 3 of~ Date (MM-DD-YY) JI Oc7 'J~ -Fie),~ Pcrsc,11.--:: C\VH, GAO Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID II ::Z:Tc:I J J ~ Weather Conditions Air Temperature oc. Total Well Depth (TWD) = Depth To Groundwater (DGW) = Length Of Water Column (LWC) = I Casing Volume (OCV) = LWC x = gal. 3 Casing Volumes = gal. = Standard Evacuation Volume Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuauon and CollecUoo Methods TB -Teflon Bailer SSB -Scainless Steel Bailer WW -Well Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)* ODOR (SUBJECTIVE)** TB SSB WW GP Other TB SSB WW GP Other Coosrams for Casmg Diameters 1.5" = 0.092 2" = 0.163 3" = 0.367 4• = 0.652 ID ?o s,;z1 "10,.Z //0 I 3 5" = 1.02 6" = 1.47 7" = 2.00 8" = 2.61 /2~ gal. FIELD ANALYSES Casing Diameter: Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 inches Casing Material: PVC -Metal Guard Pipe: PVC -Metal · No Lockiilg Cap: Y-N Protective Abutment: Y-N 'Integrity Satisfactory: y -N Well Yield: Low -Mod. -High Rtmarks· u'.)1..01? -<-~,e.. ?or\- WELL SAMPLE TIME: ~ Remarks· . . • I = CLEAR 2 = SLIGHT 3 =MODERATE 4 = HIGH .. I =NONE 2=FAtNT )=MODERATE 4=S1RONG - - -- - - -- - - - - - - - - - - -Field Data Infonnation Sheet For Groundwater SampJiog Page~of c-\ Date (MM-DD-YY) JI Ocr o/(, Field Personnel CWH, GAO Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Well ID# TTFF . Weather Conditions Air Temperature Total Well Depth (TWD) = Depth To Groundwater (DGW) - u:ngth Of Water Column (LWC) = 1 Casing Volume (OCV) -LWC x - oc . gal. 3 Casing Volumes = gal. = Standard Evacuation Volume Total Volume of Water Removed = Method of Well Evacuation Method of Sample Collection Evacuatmn aOO CoUecnon Methods TB -Teflon Bailer SSB -Stainless Steel Bailer WW -WeU Wizard GP -Grunfos Pump VOLUME PURGED (GALLONS) TIME (24 HOUR SYSTEM) pH (SU) WATER TEMPERATURE (°C.) SP. CONDUCTIVITY (UMHOS/CM) TURBIDITY (SUBJECTIVE)• ODOR (SUBJECTIVE) .. gal. TB SSB WW GP Other TB SSB WW GP Other Constants for C.asmg P1ameters 1.5• = 0.092 5• = 1.02 2" = 0. 163 6" = 1.47 3• = 0.367 1· = 2.00 4 • = 0.652 8" = 2.61 FIELD ANALYSES /03~ "'x. /0 2 t .if ,Z.3o -'?'JL/4 I I Casing Diameter: Shealy Environmental Services, Inc. 106 Vantage Point Drive Cayce, S.C. 29033 inches Casing Material: PVC -Metal Guard Pipe: PVC -Metal -No Locking Cap: y -N Protective Abutment: y -N 'Integrity Satisfactory: y -N Well Yield: Low -Mod. -High Remarks· ww,? -----n\e. ?or+ WELL SAMPLE TIME: /03~ Remarks· ' I = CLEAR 2 = SLIGIIT 3 =MODERATE 4 -HIGH .. -!=NONE 2-FAINf 3-MODERATE 4-STRONG u . • --CHAIN OF CUSTODY # Client Name I:-..~ l·,..,Q .. ,'c, <, (,.\ Cc.l'. "",,hcl\J •·.v Reporting Address ______________ _ Attention Telephone No. rfo. No. Y,. <-\ ',, ~ 0 ~ "' Sample ID (Location) TIME ~ ::; , ~ DATE w 0 0 • ,,, u " Star1 I \.) . 7.::, ,o-7:,\ \':.:>Cy y I Ftmsh Start 10-,, <":>tO ~ F,n,sh Start F,msh Start 'o-3\ 'O~r:: F1n1sh I\\? \31 i::,, <.. I'.:_ Start \Q--:2-<j' X'.2. J .. 1 I:_ 1- \/c.~ ,} , \ ca..J.\ e Star1 ,o---::,, ,..:rss F1msh I( s Start Finish &.J dV~M--L-Vlc:MIPIN .. 106 Vantage Pointe Drive Cayce, South Carolina 29033 Telephone No. (803) 791-9700 Fax No. (803) 791-9111 - - - - ~\.,~ NPDES # _____________ _ County ______________ _ CHAIN OF CUSTODY RECORD Receiving Stream ___________ _ SAMPLE ANALYSIS REQUIRED c.. y ,,. • ii ] 0 , .. ,' 0 ,~ ~ "' ,. x x y ;1. l 'i- " )1_ . K )(_ \ \ ~ ,; } Outfall No. _____________________ _ +-PRESERVATION (CODE) CODE: A = None B=HN03 C = H2S04 D • NaOH E·-rce F = Hq REMARKS fl,\ .-roe.....'"" -\-o \:i e- r..._~_,, , ,.._ V._L{l \, c....G~' _ . LAB USE ONLY Program Area (Circl~t -., OW CWAl6°t:DE§ l RCRA SP1S SP/LIO Other· __ SESI LABI.D. I r::SA=M::P::-L::ER;::-------_.J'-----,.L..--D,-Ja-t..Je/T='im_e..L..L--',----R,1-e'-c..JeLiv_ed.L..b..Jy ... (S,--iLg.-) ..L...J........J._.J_.L....L.....L,-1-'--D,1-a-t..Je/T=-imL_ .-"-L,---H-.,-.-,d-,-A-,,-oc-ia-,e-d_w .... ith-S,--a_m_p ___ le--L,-c-,-,.-,.-,-s .. -11-a1-act_(_C-ird-,-l -l 6 \ t\ f A i Print Name:~~",.,,, 1· .~ ~,c;,.,. /.l.f-1 ":,, ,, .. ,, .. .;,. '/i'r,.-:1' R"'o:,E:RC_"_O_N_O_N_E. mg/I ~ Signature: ClJ!_ -'<.ct• ... ,.: l /' :.'... ·r_. 1/f'_,(1 t:i ~ -' .. .. ., RecelptpH ____ ~'" ~ Relinquished by {Sig.) Dateffime Received by (Sig.) Date/Time t ., , U ..: ,:r'I.; ;· • ffi A I I ~ •--'-"" Rel (i'1i•1 ~ by (Sig] (/ , k. . -l(Cd..1__,,,.______ pie< Date/Time \CJ--=;\ q<.J \(\00 lab Receipt by (Sig.)~· / .::-><::.~C..t..c .. l C \-, EC,.~ : She< Date/Time \C.'-:',\-c,ti l':"'.\C'O Receipt Terri,. ____ 'C Received on Ice (Circle) (_:Es _ NO ICE PACK :opy: -------------------Inner Tier Combined Influent TOC Data ITCI TOC Data 4000~----------------------------------- 3500 ---------------------- 3000 i 2500 E -C 0 ~ 2000 ~ -C a, u 5 1500 u ----------------------------------------------------------------------------------------- 1000 ---------------------------------------------------------------------- 500 ---------------------------------- o-l---------+---------1--------------+---------+_J 1/1/93 1/1/94 1/1/95 Date 1/1/96 12/31/96 ------------------- ITCI Ethylene Glycol Data Location Qal!l. ~ l.lni1 ITCI Ethylene Glycol Data ITCI 11 /29/94 2330 mg/L J 2500 ITCI 3/7 /9 5 1800 mg/L ITCI 5/18/95 1000 mg/L JL mg/L 2000 .. ------------------------------------------ ITCI 8/22/95 209 ::, ITCI 11 /29/95 52 mg/L z 0) ITCI 1 /1 6/96 11 00 mg/L, e· ; 1500 -------------------------------------------- ITCI 4/15/96 1070 mg/L 0 ITCI 7/12/96 550 mg/L ;; .. ~ 1 0/31 /96 840 mg/L -ITCI i 1000 -------- u C 0 0 500 ------------------------------------------ 0+--------~--------+-- 11/29/94 11 /29/95 11 /28/96 Date - - - - - - - - --· - - - - - - - - - Monitor Well V-23 Acetone Data LQ~atiQ □ lla1ll. ~ l.lni1 V-23 8/3/89 0 .1 mg/L u V-23 11 /9/89 0.295 mg/L V-23 1 /5/90 0.3 mg/L V-23 2/2 3/9 0 0.34 mg/L V-23 Acetone Data V-23 8/8/90 0.31 mg/L V-23 11/7/90 0.01 mg/L u V-23 2/5/91 0.52 mg/L 1.2 V-23 5/3/91 0.53 mg/L V-23 8/9/91 0.48 mg/L 1 -- - - ----- - - ---------- -- - - ----------------------- V-23 11/4/91 0.53 mg/L ~ V-23 2/4/92 0.08 mg/L B C) E 0.8 ----- ----- ------------ - V-23 5/5/92 0.2 mg/L u -. C V-23 8/7/92 1.1 mg/L E 0 ~ 0.6 --------------- ------ V-23 11 /6/92 0.14 mg/L ~ -V-23 2/3/93 0.05 mg/L u C CD g 0.4 ------------- - - ----------- V-23 5/5/93 1 mg/L B 0 V-23 8/6/93 0.025 mg/L 0 V-23 11 /3/93 0.01 mg/L u 0.2 ----- V-23 2/2/94 0.36 mg/L V-23 8/5/94 0.52 mg/L 0 V-23 3/8/95 0.01 mg/L 6/1/89 6/1/91 5/31/93 5/31 /95 V-23 8/24/95 0.648 mg/L J Date V-23 1/16/96 0.487 mg/L V-23 7/11/96 1.15 mg/L -------------------Monitor Well K-28 TOC Data K-28 TOC Data 8000.00 ~----------------------------------, 7000.00 ----- ---- -- ------- ------------ ---- ------------------------------------------------------------ 6000.00 ---------------------------------------- -...I 0 5000.00 E -C 0 :;:: 4000.00 (II ~ -C fl g 3000.00 0 2000.00 1000.00 --- --- ------ ----- -- ----------- ------------------------------- ----- 0.00 +-4~ ...... --+-----+----+-----,,------+--__..:.:_+-_:____::::.,-+-... +:!ILI 9/1/81 9/1 /83 8/31/85 8/31/87 8/30/89 Date 8/30/91 8/29/93 8/29/95 ------------------- Monitor Well K-28 Acetone Data l,Qi.atiQD Qa1e. Y.al.u.e. lln.i.l K-28 8/4/89 0.43 mg/L K-28 11/9/89 0.159 mg/L u K-28 1 /4/90 0.074 mg/L K-28 Acetone Data K-28 2/19/90 0.39 mg/L B K-28 5/4/90 0.24 mg/L 3 K-28 8/8/90 0.074 mg/L K-28 11 /6/90 0.39 mg/L K-28 2/6/91 2.6 mg/L E 2.5 -------------------------------------------------------- K-28 5/3 /91 0.25 mg/L -K-28 8/8/91 0.082 mg/L ..J C) 2 ------------------------------------------------------- K-28 11/4/91 1.1 mg/L §. K-28 2/4/92 0.13 mg/L C 0 K-28 5/5/92 0.05 mg/L u t; 1.5 ------------------------------------------------------- ~ K-28 8/7 /92 0.2 mg/L -C 11/6/92 0.029 mg/L ., K-28 u 1 ------------ - - - - - - ----------- ----- - - ----- ---- - ---C ------ K-28 2 /3/9 3 0.068 mg/L 0 0 K-28 5/5/93 0.068 mg/L K-28 8/6/93 0.057 mg/L 0.5 ------------------------------------------------------ K-28 11/3/93 0.14 mg/L K-28 2/2/94 0.034 mg/L 0 K-28 8/8/94 0.02 mg/L 6/1 /89 6/1/91 5/31/93 5/31/95 K-28 3/9/95 0.01 mg/L < Date K-28 8/23/95 0.01 mg/L < K-28 1 /1 6/96 0.05 mg/L < K-28 7/11/96 0.02 mg/L < - - - - - - - - - - - - - --.-- - - Monitor Well K-28 Benzene Data LQi;;aliQO .l2ale. Yal.u.e. J.J.n.i.t K-28 8/4/89 0.022 mg/L K-28 11 /9/89 0.005 mg/L u K-28 1 /4/90 0.015 mg/L K-28 Benzene Data K-28 2/19/90 0.025 mg/L u K-28 5/4/90 0.018 mg/L K-28 8/8/90 0.03 mg/L 0.03 K-28 11/6/90 0.015 mg/L K-28 2/6/91 0.019 mg/L K-28 5/3/91 0.014 mg/L J 0.025 ----- --------------------------------------------- K-28 8/8/91 0.017 mg/L K-28 11/4/91 0.03 mg/L J :::. K-28 2/4/92 0.017 mg/L C) 0.02 ----- - -------- -- - ----- --------------------. ------ K-28 5/5/92 0.017 mg/L J .§.. K-28 8 /7 /9 2 0.019 mg/L C 0 K-28 11/6/92 0.009 mg/L J 'j;; 0.015 ~ K-28 2/3/93 0.009 mg/L J -C .. K-28 5/5/93 0.014 mg/L " C K-28 8/6/93 0.015 mg/L 0 0.01 u K-28 11 /3/93 0.011 mg/L K-28 2/2/94 0.014 mg/L 0.005 --------------------------------------------------K-28 8/8/94 0.018 mg/L K-28 3/9/95 0.006 mg/L K-28 8/23/95 0.0205 mg/L K-28 1/16/96 0.0086 mg/L 0 K-28 7/11/96 0.0149 mg/L 6/1/89 6/1/91 5/31 /93 5/31/95 Date ------------------- Monitor Well K-28 2-Butanone Data (MEK) l,QQaliQ□ I2a1fl Yal.u.e l.1J:J.i1 K-28 8/4/89 0.19 mg/L K-28 11/9/89 0.074 mg/L K-28 2-Butanone Data (MEK) K-28 1/4/90 0.099 mg/L K-28 2/19/90 0.28 mg/L K-28 5/4/90 0.24 mg/L 0.3 K-28 8/8/90 0.12 mg/L K-28 11/6/90 0.24 mg/L 0.25 ------------------------------------------------ K-28 2/6/91 0.04 mg/L K-28 5/3/91 0.05 mg/L u :::; 0.031 mg/L -0.2 K-28 8/8/91 "' - - - --. - ------------------------------------------- K-28 11/4/91 0.046 mg/L J .§. C K-28 2/4/92 0.094 mg/L 0 'f 0.15 - - - - - -. ------------------------------------------ K-28 5/5/92 0.05 mg/L u -K-28 8/7/92 0.071 mg/L C CD 11 /6/92 0.026 mg/L u K-28 C 0.1 0 K-28 2/3/93 0.01 mg/L u u K-28 5/5/93 0.01 mg/L u K-28 8/6/93 0.056 mg/L 0.05 K-28 11 /3/93 0.13 mg/L K-28 2/2/94 0.034 mg/L 0 K-28 8/8/94 0.011 mg/L 6/1/89 6/ 1 /91 5131/93 5/31/95 K-28 3/9/95 0.01 mg/L < Date K-28 8/23/95 0.01 mg/L < K-28 1/16/96 0.01 mg/L < K-28 7/12/96 0.01 mg/L < ------------------- Monitor Well CC-33 Benzene Data LQCaliQ □ .D..am '.'lal.u.e. llnil CC-33 8/4/89 0.085 mg/L CC-33 11/8/89 0.08 mg/L CC-33 Benzene Data CC-33 2/14/90 · 0.081 mg/L CC-33 5/4/90 0.079 mg/L o. 14 CC-33 8 /9 /9 0 0.096 mg/L CC-33 11 /6/90 0.073 mg/L 0.12 ---------------------------------------------------- CC-33 2/6/91 0.095 mg/L CC-33 5/2/91 0.089 mg/L CC-33 8/8/91 0.08 mg/L 0.1 --------------------------------------------------- ::. CC-33 11/4/91 0.14 mg/L c CC-33 2/4/92 0.11 mg/L E ;a.OB ---------- - - - ---- - - ----- - - ----- - - - - - - CC-33 5/4/92 0.11 mg/L 0 CC-33 8/7 /92 0.1 mg/L ;:; m CC-33 ~ 11 /5/92 0.086 mg/L ~ 0.06 --- - - ---------------------- CC-33 2/3/93 0.052 mg/L u C CC-33 5/5/93 0.055 mg/L 0 0 CC-33 8/5/93 0.059 mg/L 0.04 ----- -------------------- - - - -------------------------- CC-33 11 /2/93 0.055 mg/L CC-33 2/2/94 0.045. mg/L 0.02 --- - - - - - --- - - - ------- CC-33 8/4/94 0.026 mg/L CC-33 3/9/95 0.014 mg/L CC-33 8/24/95 0.0176 mg/L 0 CC-33 1/17/96 0.01 mg/L 6/1 /89 6/1 /91 5/31 /93 5/31 /95 CC-33 7/12/96 0.0128 mg/L Date CC-33 Dupe 1/17/96 0.0125 mg/L ------------------- Monitor Well CC-33 Chlorobenzene Data L,Qi;;aliQ□ llillll. ~ Uni1 CC-33 8/4/89 0.024 mg/L CC-33 11 /8/89 0.027 mg/L CC-33 Chlorobenzene Data CC-33 2/14/90 0.021 mg/L CC-33 5/4/9 0 0.019 mg/L CC-33 8/9/9 0 0.02 mg/L 0.03 CC-33 11 /6/90 0.019 mg/L CC-33 2/6/91 0.018 mg/L 0.025 --------------------------------------- CC-33 5/2/91 0.019 mg/L CC-33 8/8/91 0.015 mg/L :J' CC-33 11/4/91 0.024 mg/L D) 0.02 CC-33 2/4/92 0.017 mg/L §. CC-33 0.017 mg/L C 5/4/92 0 1ii 0.015 ------------ - - - ------ - - - - - - - - - - ---- --- CC-33 8 /7 /9 2 0.016 mg/L ~ -CC-33 11 /5/92 0.012 mg/L C .. CC-33 2/3/93 0.01 mg/L u C 0.01 ------------- - - - - - - - 0 CC-33 5/5/93 0.01 mg/L J u CC-33 8 /5 /9 3 0.011 mg/L 0.005 ------------ - - - - - ------ - --- CC-33 11/2/93 0.008 mg/L J CC-33 2 /2 /9 4 0.006 mg/L J CC-33 8/4/94 0.004 mg/L J 0 CC-33 3 /9 /9 5 0.005 mg/L < 6/1 /89 6/1/91 5/31 /93 5/31 /95 CC-33 8/24/95 0.005 mg/L < Date CC-33 1/17/96 0.005 mg/L < CC-33 7/12/96 0.005 mg/L < CC-33 Dupe 1/17/96 0.005 mg/L < ------------------- HH-48 TCE Data l,Q~ali!l□ Qa1a Ya!.u..e. J.J.ni1 HH-48 8/3/89 0.16 mg/L HH-48 11/7/89 0.14 mg/L HH-48 2/5/90 0.005 mg/L u HH-48 5/1 /90 0.17 mg/L HH-48 8/2/90 0.15 mg/L HH-48 TCE Data HH-48 11/2/90 0.15 mg/L HH-48 2 / 1 /91 0.15 mg/L 0.25 HH-48 5/2/91 0.12 mg/L HH-48 8/2/91 0.01 mg/L u HH-48 11/1/91 0.16 mg/L 0.2 · -- - -- -------------------- - - HH-48 2/3/92 0.16 mg/L ::::, HH-48 4/30/92 0.15 mg/L -C) HH-48 8/3/92 0.18 mg/L E ~ 0.15 · ---- - HH-48 11 /3/92 0.22 mg/L E C 0 HH-48 2/1 /93 0.15 mg/L = .. ~ HH-48 5/3/93 0.18 mg/L -C 0.1 ------------- ------ ---------- ---- - - --------------., HH-48 8/2/93 0.2 mg/L " C: HH-48 11/1/93 0.22 mg/L E 0 0 HH-48 1/31/94 0.2 mg/L 0.05 ----------------------- - ----- - - --------------- HH-48 8/1 /94 0.16 mg/L HH-48 8/1 /94 0.01 mg/L HH-48 3/8/95 0.17 mg/L 0 HH-48 8/23/95 0.222 mg/L 6/30/89 6/30/91 6/29/93 6/2 9/95 HH-48 1/17/96 0.165 mg/L Date HH-48 7/12/96 0.179 mg/L HH-48 DUPE 11 /3/92 0.2 mg/L D ------------------- LQi;;atir;rn D..a1ll ~ JJ..o.i.l HH-77 8/3/89 0.008 mg/L HH-77 8/2/90 0.04 mg/L HH-77 8/2/91 0.13 mg/L HH-77 8/3/9 2 0.067 mg/L HH-77 8/2/93 0.12 mg/L HH-77 8/1 /94 0.12 mg/L HH-77 8/23/95 0.332 mg/L HH-77 1/17/96 0.187 mg/L HH-77 7 /1 2/96 0.383 mg/L HH-77 TCE Data HH-77 TCE Data 0.4 0.35 -..J 0.3 -"' E -0.25 C 0 ;: 0.2 '" --i 0.15 u C 0 0.1 0 0.05 0+x.-----+------+-----t-----' 6/1/89 6/ 1 /91 5/31/93 Date 5/31/95 -------------------Monitor Well V-23 TOC Data V-23 TOC Data 12000 ,-------------------------------------, 10000 -8000 ---------------------------- ..J -C, E - 4000 2000 ----------------------------------------- 0-l-------+------+------l'-----~lq------+----------+1 1 /l/85 1/1/87 12/31 /88 12/31/90 Date 12/30/92 1 2/30/94 12/29/96 ------------------- Monitor Well V-23 2-Butanone Data (MEK) Li;u;:atiQ□ .lla1e. ~ Uni! V-23 8/3/89 1.1 mg/L V-23 2-Butanone (MEK) V-23 11 /9/89 0.45 mg/L V-23 1 /5/90 0.37 mg/L V-23 2/23/90 0.038 mg/L 4 V-23 8/8/90 0.56 mg/L V-23 11/7/90 0.01 mg/L u 3.5 ---------------------------------------------... V-23 2/5/91 0.66 mg/L V-23 5/3/91 0.46 mg/L 3 --------------------------------------------:::. V-23 8/9/91 0.04 mg/L u -CJ) V-23 11/4/91 0.05 mg/L u §. 2.5 -------------------------------------------- V-23 2/4/92 0.2 mg/L C 0 V-23 5/5/92 0.2 mg/L u = 2 ------------ --------- - - - --- - - - ------------ CD ~ V-23 mg/L -8/7/92 0.8 C fl 1.5 -------------------------------------------V-23 11/6/92 0.1 mg/L u C V-23 2/3/93 0.05 mg/L u 0 u ... . . . V-23 5/5/93 0.25 mg/L u V-23 8/6/93 0.044 mg/L 0.5 V-23 11 /3/93 0.01 mg/L u V-23 2/2/94 0.25 mg/L u 0 V-23 8/5/94 0.52 mg/L 6/1 /89 6/1/91 5/31 /93 5/31/95 V-23 3/8/95 0.01 mg/L < V-23 8/24/95 0.767 mg/L Date > V-23 1 /1 6/96 3.6 mg/L V-23 7 /12/96 0.5 mg/L