NCD003446721_19960627_Celeanse Corporation - Shelby Fiber_FRBCERCLA RA_OU-1 Operating Summary February - April 1995-OCR

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Operable Unit 1 Operating Summary
February 1995 -April 1995
Hoechst Celanese Corporation
Shelby, North Carolina
Document Control No. 026SB-0020
Submitted to
U.S. Environmental Protection Agency
Region IV
Atlanta, Georgia
Prepared for
Hoechst Celanese Corporation
Shelby, North Carolina
June 1995
Kubal-Furr & Associates
RECEIVED
JUL 03 1995
SUPERFUND SECTION
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Po.st Office Box 273210
Tampa, FL 33688-3210
813/931-7730
FAX/931-8039
Ms. Kathryn Frank
Hoechst Celanese Corporation
Shelby Plant
Post Office Box 87
Shelby, NC 28151-0087
Kubal-Furr & Associates
Environmental Consultants
June 27, 1995
Re: OU-1 Operating Summary, Feb '95-Apr '95
Document Control Number 026SB-0020
Dear Kathryn:
1120 W. Butler Rd., Suite Q
Greenville, SC 29607
803/277 -0977
F AX/277.f,626
We are pleased to submit the enclosed report entitled: "Operable Unit 1 Operating Summary,
February 1995-April 1995" This report includes the analytical test results from the quarterly
sampling event conducted between March 6-9, 1995.
The next sampling is a quarterly event which was conducted during the week of May 15-19,
1995, with the next operating summary report to be submitted in September 1995.
Sincerely,
Kubal-FwT & Associates #~w_
. Jerry 'ft-Kubal
· . Licensed Geologist
(NC License No. 212)
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Contents
Page
Inuuduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Work Performed ................................................ 2
System Performance .............................................. 6
Discussion of Water Quality Findings ................................... 9
Quality Assurance Summary ...................................... 9
Domestic Supply Wells ......................................... 9
Monitor Wells ............................................... 10
Inner/Outer Tier Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
Other Test Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
Closing Comments .............................................. 14
Tables
Table l. Quarterly Sampling Matrix .................................... 4
Table 2:. Inner Tier Prcxiuction Data (Feb '95-Apr '95) ....................... 7
Table 3. Outer Tier Production Data (Feb '95-Apr '95) ....................... 8
Table 4. Inner/Outer Tier TOC Data (Feb '95-Apr '95) . . . . . . . . . . . . . . . . . . . . . . . 13
Attachments
Attachment I. February 1995 Operation and Maintenance Data
Attachment 2. March 1995 Operation and Maintenance Data
Attachme:nt 3. April 1995 Operation and Maintenance Data
Attachment 4. Data Quality Assessment Summary Repon
Attachment 5. Water-Level Measurements, Sampling Logs, Chrun-of-Custcxiy Forms
Attachment 6. Analytical Data for the March 6-9, 1995 Sampling Event
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Introduction
Hoechst Celanese Corporation (HCC) is currently operating a long term remedial action
(L 1RA) system at its Shelby, North Carolina facility. This system, designated as Operable Unit I
(OU-1) in the Record of Decision, consists of two ground-water extraction and treatment systems:
the Inner Tier and the Outer Tier. OU-I became operational in August 1989.
Kubal-Furr & Associates (KF&A) has prepared this operating summary report for submittal to
the EPA on behalf of HCC. It covers the period from February 1, I 995 through April 30, 1995
and includes information on system performance and the results of analytical testing of samples
collected between March 6-9, 1995.
Kubal-Furr & Associates/Page 1
OU-1 Operating Summary (Feb '95-Apr '95)
Hoechst Celanese Corporation------Shelby, North Carolina
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Work Performed
As part of the OU-1 remedy, samples are collecied at selected monitor wells, domestic supply
wells, and at points in the ground-water treatment system. The frequency of analysis and the
parameters to be analyzed are contained in the OU-1 Five Year Review Report dated August 8,
1994.
On March 3, 1995, a letter request was submitted to the EPA to set aside the requirements for
analytical testing using CLP (contract laboratory program) protocols for routine quarterly
monitoring under the L TRA program. The request was to continue to analyze samples using the
same SW-846 test methods but to delete the requirements for CLP protocols and deliverables. The
EPA provided verbal concurrence with the request on March 8, 1995, followed by written
approval on March 28, 1995.
During the current reporting period, the scope of work consisted of the semiannual sampling
program. Samples were collected at the locations and analyzed for the parameters summarized in
Table 1. Samples were collected from 5 domestic supply wells, 26 monitor wells, and 6 process
points. These samples were collected by IEA Laboratories of Raleigh, NC. IEA also performed the
analyses with the exception of the total organic carbon (TOC) which is analyzed by the HCC on-
site lab.
The Lambert, Crotts (formerly the Walker residence), Stein, and Runyans wells were analyzed
in the field for pH, temperature, and conductivity; for TOC by EPA Method 415.1; for chromium
by EPA Method 6010; for TCL (target compound list) volatile organics by EPA Method 8240; for
DW (drinking water) volatile organics by EPA Method 502.2; for DW semivolatile organics by
EPA Method 525; and for DW pesticides and PCBs by EPA Method 505. The Elliott well was
analyzed for DW volatiles, semivolatiles, pesticides and PCBs by the 500-series drinking water
methods described above.
Several modifications to the sampling and analysis program occurred this reporting period with
respect to tJ1e dom~stic supply wells. These ~terns included the following:
• In accordance with the OU-1 Five Year Review Report (RUST, August 1994), the State of
North Carolina, with EPA concurrence, requested that the domestic supply wells be
analyzed by the 500-series drinking water methods in order to achieve lower detection
Kubal-Furr & Associates/Page 2
OU-I Operating Summary (Feb '95-Apr '95)
Hoechst Celanese CorporaJion-Shelby, Norch Carolina
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limits. This addition was made for the Lamben, Crotts (Walker), Stein and Runyans wells.
Maintaining a program established some time back, these wells also were analyzed for
volatile organics by the EPA SW-846 Test Method 8240.
• In prior samplings, the Elliott well was only analyzed for trichloroethylene and vinyl
chloride. In order to provide comparable and consistent test results for the domestic supply
wells, the Elliott well was analyzed by the same 500-series drinking water test methods for
volatiles, semivolatiles and pesticides. It was not, however, analyzed for volatiles by EPA
Method 8240.
• It was discovered during this sampling period that the Runyans residence (located adjacent
to and just southwest of the Lamben propeny), rather than Martin residence, has been the
domestic supply well sampled for at least the past few years. The Runyans sample has been
mistakenly identified as the Martin residence on the water sampling forms, chain-of-
custody forms, and analytical test results for some period, and HCC is attempting to
establish when this change occurred. Apparently, a recommendation to switch from the
Manin residence to the Runyans residence was made at the time the Runyans moved to the
site. Although no formal approval by the EPA authorizing this change has been found, the
laboratory at some point began collecting samples from the Runyans well, while still
referring to it as the Martin residence. An attempt to resolve this issue will be conducted
during the next reporting period
In addition to the domestic well samples, samples were also collected from selected monitor
wells, the extraction wells and the treatment systems. The monitor wells were analyzed for TCL
volatiles and/or TOC. One sample each of SBR (Sequencing Batch Reactor) wasted sludge and FP
(filter press) sludge were analyzed for full TCLP. The SBR sample was also analyzed for TCL
volatiles, semi volatiles, pesticides and metals.
Samples of Inner Tier (IT) influent and effluent, and Outer Tier (OT) influent and effluent were
collected for analysis of TOC, and TCL volatiles. The Inner Tier influent and effluent samples
were also analyzed for TCL semivolatiles, pesticides, metals, and for ethylene glycol.
Influent and effluent samples from the Inner Tier and the Outer Tier were also collected by
HCC for analysis of TOC by the HCC on-site laboratory. These samples are collected weekly in
accordance with the schedule established in the OU-I Five Year Review Repon.
Kubal-Furr & Associates/Page 3
OU-I Operating Summary (Feb '95-Apr '95)
Hoechst Celanese Corporation------Shelby, North Carolina
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Sample
Location
AA-54
CC-33
EE-58
FF-34
FF-62
GG-61
HH-48
K-28
P-58
T-35
V-23
C-49
CC-64
D-35
D-56
FF-23
GG-25
GG-39
J-28
J-59
K-58
N-29
N-53
0-25
T-17
T-58
Table 1. Sampling Matrix-Hoechst Celanese-Shelby, NC
1st Quarter 1995 Quarterly Sampling Event
TOC pH/Temp/ Full
(415.1) Cond TCLP
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
✓ ✓ -
voes SVOCs Metals Ethylene
(8240) (8270) (6-7000) glycol
✓ ---
✓ ---
✓ ---
✓ ---
✓ ---
✓ ---
✓ ---
✓ ---
✓ ---
✓ ---
✓ --✓
✓ ---
----
----
----
----
----
----
----
----
----
----
----
----
----
----
Kubal-Furr & Associates/Page 4
OU-1 Operating Summary (Feb '95-Apr '95)
Hoechst Celanese Corporation-Shelby, North Carolina
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Table 1 (cont'd). Sampling Matrix-Hoechst Celanese-Shelby, NC
1st Quarter 1995 Quarterly Sampling Event
Sample TOC Full TCLP voes SVOCs Pest. Metals Ethylene
Location (415.1) (8240) (8270) (8080) (6-7000) glycol
OTinf ✓ ✓
OTEff ✓ ✓ ✓ ✓ ✓
IT Inf ✓ ✓ ✓
ITEff ✓ ✓ ✓ ✓ ✓ ✓
SBR W. ✓ ✓ ✓ ✓ ✓ Sludge
FP Sludge ✓
Sample pH/Temp/ Chrom voes voes SVOCs Pest/PCB
Location TOC Cond (6010) (8240) (502.2) (525) (505)
Lambert ✓ ✓ ✓ ✓ ✓ ✓ ✓
Crotts ✓ ✓ ✓ (Walker) ✓ ✓ ✓ ✓
Stein ✓ ✓ ✓ ✓ ✓ ✓ ✓
Runyans ✓ ✓ ✓ ✓ ✓ ✓ ✓ (see Note)
Elliott ✓ ✓ ✓
Note: This well has e"oneous/y been refe"ed to as che Marrin well in several earlier repons. It is
inco"ecrly labelled on the sampling logs, chain-of-custody forms, and in the analytical dara
repons.
Kubal-Furr & Associates/Page 5
OU-I Operaiing Summary (Feb '95-Apr '95)
Hoechst Celanese Corporation-Shelby, North Carolina
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System Performance
Detailed records of system maintenance are kept by HCC and are summarized monthly. The
monthly records for the current reporting. period are contained in Attachments 1, 2, and 3.
Summaries of physical operating data for the Inner and Outer Tier extraction well systems are
presented in Tables 2 and 3, respectively.
During the reporting period, the Inner Tier wells extracted a total of 194,072 gallons, a
decrease of about 13% from the previous reporting period. Inner Tier flows ranged from a low of
53,148 gallons in April to a high of77,065 gallons in March
The Outer Tier wells extracted 7,595,980 gallons during this reporting period, a decrease of
less than 1 % from the previous reporting period. The flow from the Outer Tier system was fairly
constant, ranging from 2,316,548 gallons in February to 2,644,231 gallons in March.
No unusual operational problems were experienced during the reporting period in the Outer
Tier recovery well system with the exception of well OT-1 which was serviced on 7 occasions for
cleaning of the strainer and screens. Low flow from the Inner Tier wells is a chronic problem
requiring frequent maintenance. Wells IT-6, IT-8 and IT-9 were down for maintenance for several
days each during the reporting period. The actions taken to rectify the low flow problems consisted
of replacing bladders, timers, air lines and such, adjusting the controls and flow rates and cleaning
the strainers. Specific actions taken at individual wells during the reporting period are contained in
the monthly operating summaries (Attachments 1, 2, and 3).
Kubal-Furr & Associates/Page 6
OU-/ Operating Summary (Feb '95-Apr '95)
Hoechst Celanese Corporaiion----Shelby, North Carolina
February 1995
Table 2. Inner Tier Production Data
Feb '95-Apr '95
Hoechst Celanese Corporation-Shelby, NC
March 1995 April 1995
Well Total Gallons ADF• Total Gallons ADF•
213
58
Total Gallons
6,647
2,137
ADF•
222
7 1
Total Gallons
IT-1 6,034 216
IT-2 1,764 63
IT-3 ...................... 5_..023 ................... 179
IT-4 3,879 139
IT-5 9,127 326
6,605
1,794
19,286
5,695
6,398 206 4,934 164 16 355 ---················ .. ···•• .. •••····•····•·• .......................................................................................................................................... 1 ............ .
7,495 242 6,361 212 17,735
9,610 310 5,436 1 81 24,173
IT-o 4134 ................................................... 148 4,337 140 2,896 97 11 367 ................................................................................................................................................................................................................................................ 1.. .......... .
IT-7 4,339 155 6,116 197 4,773 159 15,228
IT-8 4,435 158 6,450 208 5,314 177 16,199
IT-9 25,124 897 28,260 912
63,859 77,065
• ADF: Average Daily Flow based on HCC production records (Attachments 1, 2, 3)
Calculated as total flow divided by the number of days in the month.
14,650 488 68,034
53,148 194,072
--~--------~-------
wen
OT-1
OT-2
Table 3. Outer Tier Production Data
Feb '95-Apr '95
Hoechst Celanese Corporation-Shelby, NC
February 1995
Total Gallons
577,600
696,661
ADF*
20,629
24,881
March 1995
Total Gallons
654,100
758,040
ADF*
21,100
24,453
Aprll 1995
Total Gallons
620,900
836,156
ADF'
20,697
27,872
Total Gallons
1,852,600
2,290,857
OT-3 57,086 2039 65,629 2,117 62,610 2,087 185325 :...=. __ ........................................................... ! ....................................................................................................................................................................................................................... , .......... ..
OT-4 30,598 1,093 40,767 1,315 43,861 1,462 115,226
OT-5
OT-6
OT-6A
OT-7
OT-8
72,095
1 72, 74 7 ..........
172,605
70,456
466,700
2,316,548
2,575 70,437
6,170 ······················208,891
6,164 206,671
2,516 77,796
16,668 561,900
2,644,231
2,272 68,076 2,269 210,608
6,738 210,918 7,031 592 556 .................................................................................................................. , ...........
6,667 198,161 6,605 577,437
2,510 85,919 2,864 234,171
18,126 508,600 16,953 1,537,200
2,635,201 7,595,980
• ADF: Average Daily Flow based on HCC production records (Attachments 1, 2, 3).
Calculated as total flow divided by the number of days in the month.
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Discussion of Water Quality Findings
The analytical test results for the current reporting pericxi were evaluated using the methcxi
specific quality control criteria and the EPA's National Functional Guidelines for laboratory data
validation. The data quality assessment summary report for this sample set is contained in
Attachment 4. Water-level measurements, field sampling logs, and chain-of-custody forms are
provided in Attachment 5. The analytical test results for this reporting pericxi are contained in
Attachment 6.
Data Qus11ity Assessment
TCUTCLP Volatile Organics (Method 8240)
The TCLP volatile fraction for the SBR sludge was discarded by the laboratory without being
analyzed. The non-TCLP SBR sludge sample, however, was analyzed for the TCL volatiles by
Methcxi 8240. All TCL and TCLP volatile data are considered quantitative and useable.
Drinking Water Volatile Organics (Method 5022)
The positive results from the Runyans (Martin) sample are flagged "JK" (estimated, biased
high) due to high surrogate recoveries in the spike sample. All other drinking water volatile data are
considered useable for all purposes as quantitative data.
TCLffCLP Semivolatile Organics (Method 8270)
Due to low surrogate spike recoveries, positive results for the FP sludge and the FP spike are
flagged "J" (estimated), while non-detect results are flagged "UJL" (estimated quantitation, results
biased low). Due to out of control matrix spike and matrix spike duplicates, positive results for the
SBR sludge and OT Eff samples are flagged "JK" (estimated, biased high). All other semivolatile
data are considered useable for all purposes as quantitative data.
Drinking Water Semivolatile Organics ( Method 525)
The pentachlorophenol results (all non-detect) for all wells are flagged "UJL" (estimated
quantitation, results biased low) due to low surrogate spike recoveries and/or out of specification
Kubal-Fu" & Associates/Page 9
OU-I Operating Summary (Feb '95-Apr '95)
Hoechst Celanese Corporatio~he/by, North Carolina
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percent differences for continuing calibration. The semivolatile data for the Runyans (Martin) well
(all non-detect) are also flagged "UJL" due to low surrogate recoveries outside the control limits,
suggesting a matrix interference. All other semivolatile data are considered useable for all purposes
as quantitative data.
TCLrfCLP Pesticides!PCBs (Metlwd 8080)
All pesticide/PCB results were reported as non-detect. Results for several constituents were
flagged as "U l" (not detected, but compound not calibrated in performance of the method by the
lab); "UJ" (not detected, but continuing calibration out of specification); or, "UJL" (not detected,
but laboratory control samples outside of control limits).
Drinking Water Pesticides (Metlwd 505)
All pesticide results were reported as non-detect. Results for numerous constituents were
flagged ''UJL" (not detected, but relative standard deviations out of control in initial calibration);
"UQ 1" (not detected, but results obtained by a method other than that specified); or, "UQ2" (not
detected, analytical methodology suspect).
TAL!TCLP Metals (6000-7000 Series Metlwds)
Sample IT Eff is flagged "JL'' (estimated quantitation, biased low) because the sample was not
properly preserved. It was received by the laboratory at a pH of 7 and should have been <2.0.
Also, aluminum, copper and nickel results for this sample are reported as non-detect due to their
presence in laboratory calibration and preparation blanks. All other metals data are considered
useable for all purposes as quantitative data.
Domestic Supply Wells
With the exception of acetone (at 11 µg/L) in the Runyans (Martin) well, no volatile organics
above the detection limits were reported with Method 8240 in any of the domestic supply wells.
The constituents benzene, at 1.3 µg/L, and 1,2-dichloroethane (1,2 DCA), at 7 .8 µg/L, were
reported as present in the Runyans well using the 502.2 drinking water test method. As discussed
Kubal-Furr & Associates/Page 10
OU-/ Operating Summary (Feb '95-Apr '95)
Hoechst Celanese Corporation-Shelby. North Carolina
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in the data assessment section, these constituents are considered present but biased high due to
high surrogate recoveries in the spike sample.
"The laboratory was asked to review the chromatograms for the 8240 analyses for the Runyans
well to see if any peaks were evident for benzene or 1,2 DCA. IEA indicated that no 1,2 DCA
peak was present but that there was some evidence that benzene was present, but below the
quantitation limit of 5 µg/L.
The 502.2 test results for acetone, benzene and 1,2 DCA are above the North Carolina
Ground-Water Quality Standards specified in Title 15, Subchapter 2L. Acetone has routinely been
reported as present in the IEA laboratory blanks. It was qualified in the previous reporting period,
and its reported presence here is most probably as a laboratory artifact.
While there is no Federal Primary Drinking Water Standard MCL (maximum contaminant
level) for acetone, the test result for benzene is below the MCL of 5 µg/L. Although the 1,2 DCA
(at 7.8 µg/L) was above the Federal MCL of 5 µg/L, this result was qualified as biased high and
was not detected with the 8240 methodology and therefore it may or may not actually be above the
MCL. One point to note in comparing the analytical results to the drinking water standards for the
Runyans well is the fact that this well is not used as a potable source of supply. The Runyans are
hooked up to County water, which they use for domestic and potable purposes.
The EPA was notified of these test results during an on-site meeting in Shelby on May 12,
1995. At the time, the analytical test results had not been validated and they were presented to the
EPA as provisional data. During the meeting, the EPA was apprised of HCC's plans to notify the
affected residents of these latest findings and of a proposal to resarnple these wells the following
week (May 15-20, 1995) to confirm the test results.
The resampling, which included splitting samples with another laboratory (Shealy
Environmental Services of Columbia, SC), occurred during the following week as planned.
Complete data packages for this sampling event were not available at the time of this report
although IEA did report verbally that benzene (at 1.4 µg/L) and 1,2 DCA (at 0.7 µg/L) were
confirmed present in the Runyans well; both constituents were reported at concentrations below the
Federal MCL of 5 µg/L. These data will be presented in the next quarterly report along with a
discussion of HCC' s activities in notifying the surrounding residents.
Kubal-Fu" & Associaies/Page 11
OU-1 Operaiing Summary /Feb '95-Apr "95)
Hoechst Celanese Corporation-----Shelby. North Carolina
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No other constituents (semivolatiles, pesticides/PCBs, or chromium) were reported as present
above the detection limits in any of the domestic supply wells. The TOC analyses performed by
HCC were consistent with previous data, and ranged from 0.813 ppm (parts per million) in the
Crotts (Walker) well to 1.180 ppm in the Runyans (Martin) well.
Inner/Outer Tier Data
The results of weekly analysis of TOC in Inner and Outer Tier influent and effluent samples are
summarized in Table 4. The reduction of TOC through the Inner Tier treatment system is consistent
with historical data, ranging from 93% to 99%, with an average reduction during the reporting
period of 98%
Outer Tier TOC reductions are also consistent with previous data but are substantially less than
the Inner Tier in terms of percentage of reduction. Outer Tier reductions ranged from 13% to 55%,
with an average during the reporting period of 43%. In one instance (February 16, 1995), the
Outer Tier effluent TOC was reportedly higher than the influent sample (27.4 mg/L vs. 9.9 mg/L).
This unusual set of sampling results has occurred several times in the past and may be related to
flow through and residence time in the system.
The percent reduction of TOC through the Outer Tier treatment system is not as high as that for
the Inner Tier because of the much lower Outer Tier influent TOC. The Outer Tier influent is
generally less than the Inner Tier effluent to begin with, and the system will never achieve the
percentage reductions found in the Inner Tier. The Outer Tier appears to be reducing TOC as well
as can be ,~xpected.
Regarding TCL volatiles, several organics constituents were reported as present in the Inner
Tier influent sample. Applying the 2-fold dilution factor to the results, the Inner Tier influent
reportedly contained acetone (110 µg/L), carbon disulfide (8.5 µg/L), 2-butanone (18 µg/L),
benzene ( 18 µg/L) and chlorobenzene (8.5 µg/L). These constituents were all below the detection
limits in the Inner Tier effluent sample. No volatiles above the detection limits were reported as
present in either the Outer Tier influent or effluent sample.
The Inner and Outer Tier effluent samples were also analyzed for the presence of semi volatile
organics by Method 8270,for pesticides by Method 8080, and for metals by the 6000-7000 series
Kubal-Furr & Associaies!Page 12
OU-1 Operating Summary (Feb '95-Apr '95)
Hoechst Celanese Corporation-Shelby, North Carolina
-------------------
Date
2/2/95
2 /9 /9 5
2/16/95 ...................................................
Table 4 .. Inner/Outer Tier TOC Data .
Feb '95-Apr '95
Hoechst Celanese Corporation-Shelby, North Carolina
(all results reported in mg/L)
Inner Tier Outer Tier
Influent Effluent % Reduction Influent Effluent
1407 71 4.6 4
% Reduction
1 3
3306 152
95
95
93
26.9 14 48
1413 101 . .......................... ~--·························································· 9 . 9 ........................ ?.?..:.~ ..................................................... .
2927 48 2/23/95 98 15.8 11 .9
17.4
25
55 1 712 59.1 3/2/95 97 38.8
........... 3/8./9 5 ...................... 1 .7.94 ........................... 4_3c..c..c·9 __ ..................... !J.~ ........... ··························1·:.1. .............. --·······························································
3/1 6/95
3/23/95
3/30/95
4/6/95
4/13/95
4/20/95
4/27/95
Average:
2006 39.8 98 9.2
2114 26.5 99 5.6
4.2
3.9
54
30
1999 ~~--········30.4 ................................. 9.8 ........................................ .!.. ............................... 3 ... 7 ................................. :l .. T .............. .
3566 51.4 99 5.8 3.5 40
3053 49 98 6.1 4.1 33
1671 28.4 98 2.9 2.3 21
3014 26.4 99 4 3.2 20
2306 56 98 1 2 7 43
Note: Outer Tier Average Influent, Effluent, and Percent Reduction do not include 2/16/95 and 3/8/95 data
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I
I
I
I
I
I
D
I
methcxls. No semivolatile organics or pesticides were reported as present above the detection limits
in either of these two samples. As noted in the quality assurance summary, the Inner Tier effluent
sample reported the presence of calcium, iron, magnesium, manganese, and sodium but the sample
was not properly preserved and the results are qualified as biased low. The Outer Tier effluent
sample reported the presence of these same metals plus potassium and zinc.
The Inner Tier influent and effluent samples were also analyzed for the presence of ethylene
glycol. The influent sample was reported to contain 1800 mg/L ethylene glycol, while the effluent
sample contained no ethylene glycol above the quantitation limit of 10 mg/L. These results are
consistent with results for the previous reporting period.
Monitor Well Data
The monitor well samples were analyzed for the presence of TOC by the HCC on-site
laboratory. Tbe highest TOC concentrations were reported at monitor wells V-23 (4085 ppm) and
K-58 (2324 ppm). These wells are adjacent to the remediated OU-2 source area and they have
historically had the highest TOC concentrations. Other monitor wells reported TOC concentrations
2 to 3 orders of magnitude less than that found at V-23 and K-58.
The monitor well samples were also analyzed for TCL volatiles by Method 8240. Only 4 of the
12 monitor wells reported the presence of any volatiles above the detection limits, and then for only
one constituent each. These included HH-48 with trichloroethene (TCE) at 170 µg/L, T-35 with 2-
butanone at 1.2 µg/L, CC-33 with benzene at 14 µg/L, and K-28 with benzene at 6 µg/L. TCE is
routinely reported as present in the HR-cluster, and benzene is the most commonly found volatile
organic at the site. While 2-butanone (aka Methyl ethyl ketone) has been reported in the past, it is a
common laboratory solvent and it is possibly an artifact. With the exception of the 2-butanone, no
un_usual or unsuspected constituents were identified in the monitor well samples during the
reporting period.
Other Test Results
Two other analyses were performed this reporting period: full TCLP on the SBR wasted
sludge and FP (Filter Press) sludge, and analysis of ethylene glycol at monitor well V-23. No
semivolatiles, pesticides, or herbicides were reported as present in either the SBR of FP sludge
samples. No volatiles were detected in the FP sludge sample, while the volatile fraction of the SBR
Kubal-Furr & Associates/Page 14
OU-I Operating Summary (Feb '95-Apr '95)
Hoechst Celanese Corporation-Shelby, North Carolina
I
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sample was discarded by the laboratory and not analyzed. As noted earlier, the corresponding SER
sample analyzed for the full TCL list of volatiles by Method 8240 did not detect the presence of
any volatiles. No TCLP metals above the detection limits were reported as present in either the FP
or SER sludge samples.
Ethylene glycol was reported at a concentration of 2900 mg/L in the monitor well V-23 sample.
This compares with an estimated concentration of 7700 mg/L reported in the previous sampling
period ..
Kubal-Furr & Associates/Page 15
OU-I Operaiing Summary (Feb '95-Apr '95)
Hoechst Celanese Corpora/um-Shelby, North Carolina
I
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Closing Comments
The extraction well production data and the analytical test results for the monitor wells and
process points were generally found to be consistent with historical information, and no unusual or
unsuspected constituents were identified during the reporting period. This sample set was the first
occasion to analyze the domestic well samples using the drinking water 500-series test methods
which have much lower detection limits than the SW-846 test methods previously approved for
use.
Low levels of two volatile organics (benzene at 1.3 µg/L and 1,2 DCA at 7.8 µg/L) were
reported as present in the Runyans well using the 502.2 test method. These constituents were
below the d,~tection limits in a second sample analyzed by Method 8240 although acetone was
reported as present at 11µ/L. Acetone has routinely been reported as present in the IEA laboratory
blanks. It was qualified in the previous reporting period, and its reported presence here is most
probably as m laboratory artifact
The Runyans well was resampled during the week of May 15-19, 1995. A verbal report from
the laboratory confirmed the presence of benzene (at 1.8 µg/L) and 1,2 DCA (at 0.7 µg/L), with
both constituents below the Federal MCL of 5.0 µg/L.
It was discovered during the reporting period that the Runyans well has been sampled for
some period of time and erroneously identified by the laboratory as the Martin residence. It was
noted that the Runyans are hooked up to County water and do not use their well as a potable source
of supply. HCC is currently researching the Runyans/Martin switch and this information will be
presented in the next quarterly report along with HCC's activities to notify the surrounding
residents of the monitoring results using the new analytical test method.
Kubal-Fu" & AssociaJes/Page 16
OU-I Operaiing Summary (Feb '95-Apr '95)
Hoechst Celanese Corporaiion---She/by, North Carolina
--
NNERTIER
DAILY FLOW:
Fml.W'Y
1995: IT-1
02/01/95 245
02/02/95 256
02/03/95 49
02/04/95 187
02/05195 190
02/06/95 260
02/07/95 272
02/08/95 192
02/09/95 253
02/10/95 260
02/11195 228
02/12/95 192
02/13/95 228
02/14195 216
02/15/95 235
02/16/95 121
02/17/95 228
02/18/95 224
02/19/95 208
02/20/95 224
02/21195 224
02/22/95 178
02/23/95 227
02/24/95 244
02/25/95 231
02/26/95 213
02/27/95 224
02128/95 225
AVG:
TOT:
216
6034
-
IT-2
76
73
14
69
78
67
68
61
63
66
57
56
58
80
41
24
53
56
57
65
69
59
75
82
79
78
80
82
63
1 764
-
IT-3
143
146
27
148
150
144
150
145
150
153
14 7
138
135
135
280
177
372
363
229
200
175
51
257
190
180
187
177
318
179
5023
- -
WELLS.WK1
IT-4
172
169
34
119
144
141
138
161
155
153
135
152
140
97
141
77
0
36
103
109
123
112
488
154
142
155
175
154
139
IT-5
423
402
80
145
158
161
237
138
495
542
445
215
294
540
478
185
453
501
513
510
2BB
344
289
204
340
275
250
242
328
IT-6
228
222
43
199
225
213
215
205
219
223
208
191
191
183
175
81
174
197
203
214
171
174
147
54
67
142
226
231
179
3879 9127 4134
-
188
185
36
177
202
197
204
BO
186
212
194
179
1 83
178
162
58
161
177
181
184
1 25
164
192
135
0
0
199
223
155
4339
-
IT-8
255
257
49
213
278
24
0
3
0
3
3
2
267
228
109
71
178
208
212
119
211
200
234
291
271
246
259
256
158
-
IT-9
1213
1199
229
1034
1201
1141
1 216
372
0
1027
1042
978
988
932
812
282
835
938
959
994
1028
905
5
1141
121 0
1102
1178
1187
897
4435 25124
2312
- - -
OUTERlER
DAILY FLOW:
eHRWlY
1995: OT-1
02/01/95 20200
02/02/95 20400
02/03/95 20400
02/04/95 20600
02/05/95 20700
02/06/95 20700
02/07/95 20900
02/08/95 20400
02/09/95 20400
02/10/95 20500
02/11 /95 19900
02/12195 20300
02/13/95 20400
02/14/95 20200
02/1 5/95 20200
02/16/95 20000
02/1 7/95 20400
02/18/95 19800
02/19/95 19900
02/20/95 20300
02/21/95 21000
02/22/95 21200
02/23/95 21200
02/24/95 21100
02/25/95 22000
02/26/95 21900
02/27/95 21000
02/28/95 21600
AVG: 20629
-
OT-2
25952
26459
26781
27345
27036
27248
27653
27219
26766
26788
25620
26225
26645
28400
26390
25933
26066
25388
26197
12109
22111
21125
21583
21937
23325
23507
22919
23936
24881
- -
WELLS.WK1
OT-3
2035
1956
2019
2047
2047
2035
2057
2030
2051
2052
2020
2039
2048
2028
2048
2047
2087
2031
2061
2053
2054
1995
2085
2072
2109
1992
2016
1972
OT-4
1131
1075
11 07
1134
11 25
210
0
0
952
11 21
1166
1172
1180
1185
1225
1210
1252
1245
1276
1305
1315
1268
1322
1335
1351
1360
1288
1286
OT-5
2737
2755
2727
2756
2769
2771
2801
271 7
2681
2676
2619
2638
2614
2558
2531
2467
2485
2373
2384
2452
2448
2492
2467
2498
254 7
2480
2326
2328
-
6563
6304
6666
6721
6733
6650
6703
6606
6676
6670
6549
6665
6689
6599
8663
6657
6764
6620
6405
398
6595
6497
6764
6649
6714
6025
7184
2039 1093 2575 6398
-
OT-6A
3809
28 73
551 7
5718
5758
5775
5813
6237
6225
6192
6043
6135
6124
5952
5941
5839
5968
5790
5891
6120
6860
7035
7165
7300
7903
7694
7462
7466
6164
--
OT-7
2518
2426
2536
2562
2557
2514
2537
2500
2522
2528
2482
2518
2530
2498
2526
251 7
2563
2501
2534
2509
2513
2420
2558
2505
2522
2513
24 78
2569
OT-8
18600
20900
8600
18800
19100
19200
19300
18900
19000
18900
18600
19000
18900
18700
18800
18400(
18900
18400
18600
19200
19100
1900
21800
14200
19500
4900
16500
2516 17285
TOT: 577600 696661 57086 30598 72095 172747 172605 70456 466700
83580
---- - - -- -- - - ---- ---
ITMAINT1.WK1
MAINTENANCE ACTIVITIES-GROLR'-IOWATER OPERABLE UNIT #1
INf\ER TIER SYSTEM
ACTION
DATE LOCATION PRC81.EM DATE ACTION MEG--WIC
02/07/95 IT-8 LOW FLOW 02/08/95 REPLACED HEA TEA .PPP
INSDE WELL COVER
02/10/95 PfWETER CAUBRATK)N 02/13/95 CALIBRATED "' 02/16/95 DOBLO\VER ELECTRICAL FALUAE 02/ 16/95 FE SET BLOWER CM
02/20/95 IT-4 LOW FLOW 02/21/95 REPl.ACED BL.ADOER .PPP
0 2/20/9 5 IT-8 LOW FLOW 02/21/95 a..EANEDBU381..ER1UPE .PPP
02/22/95 IT-3 LOW FLOW 02/22/95 REPI...J\CED BLADDER .PPP
02/22/95 IT-5 LOW FLOW 02/22/95 REPLACED BLADDER .PPP
02/24/95 IT-8 LOW FLOW
02/24/95 IT·9 LOW FLOW
02/27/95 IT-7 LOW FLOW 02/27/95 FEPAIRED BROKEN AIR .PPP
Ll'E
Paga 1 ol 1
-- -- - - -- -- - - - - ---- -
OTMAINT1.WK1
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNrT #1
OJTERTER SYSTEM
ACTION
DATE LOCATIQf', PFO'l-E.~ DATE ACTION MEOW<IC
02/03/95 OT-1 STPAN:A 02/03/95 a.EANED STRAINER ..l'PP
02/03/95 OT-4 FLOW 0 2/03/95 SET FLOW TO 2.3 GPM ..PPP
02/03/95 OT-6A FLOW 02/03/95 SET FLOW TO 4.5 GPM ..PPP
02/07/95 OT-4 LOW FLOW
02/07/95 OT-6A LOW FLOW 02/08/95 SET FLOW TO 4.9 GPM ..PPP
02/17/95 OT-4 LOW FLOW
02/17/95 OT-1 SfRAl'EA 02/1 7/95 a.EANED STRAINER ..PPP
02/17/95 OT-2 SfRA>EA 02/17/95 Cl.EANE:0 STRAIM:R ..PPP
02/20/95 OT-6 LOW FLOW 02/21/95 FEPI..ACED FLOW METER ..PPP
02/20/95 OT-BA LOW FLOW 02/21/95 SET FLOW TO 5.3 GPM .PPP
02/21/95 OT-1 STAAi-ER 02/21/95 a...EAf'ED STRAlf'ER .PPP
02/21/95 OT-2 LOW FLOW 02/21/95 a...EAf'ED STAAlf\ER
ADJUSTED FLOW TO 16 GPM
02/23/95 OT-8 LOWFlOW 02/23/95 SETFLOW .PPP
02/24/95 OT-1 SfAMEA 02/24/95 Cl..EAfED STRAIT'ER .PPP
02/27/95 OT-1 srRANSR 02/27/95 a.EAP'ED STRAlr-EA .PPP
02/27/95 OT-6 LOW FLOW 02/27/95 SET FLOW TO 5.1 GPM .PPP
02127195 OT-8 srRMER 02/27195 a..ENED STAAfl',ER .PPP
Pege 1 of 1
---- - -
RAINFALLWK1
GROl.JMJWATERMONTH... Y MONITORING:
RAINFALL DATA
DATT'
02/01/95
02/02/95
02/03/95
02/04/95
02/05/95
0 2/0 6/9 5
02/07195
02/08/95
D2/09/95
02/10/95
02/11/95
02/12/95
02/13/95
02/14/95
02/ 15/95
02116/95
02/17/95
02/18/95
02/19/95
02/20195
02/21/95
02/22/95
02/23/95
02/24/95
02/25/95
02/26/95
02/27/95
02/28/95
TOTAL
AVG
lNCltSIUAY
0.00
0,00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.30
0.00
0.00
0.00
0.40
1.50
1.90
0.50
0.10
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.80
0.40
5.90
0. 74
Page 1 of 1
- -- -- -- --- ---
----
GROUNOWATERMONTI-ll Y MONITOR~:
MER TIER COMBINED INFLLENT
PAGEr-D.1
FEB.1995
DATE:
02/01/95
02/02/95
02/03/95
02/04/95
02105/95
02/06/95
02/07195
02/08/95
02/09/95
02/10/95
02/11/95
02/12/95
02/13/95
02/14/95
02/15/95
02/16/95
02/17/95
02/18/95
02/19/95
02/20/95
02/21/95
02/22/95
02123/95
02/24/95
02125/95
02126/95
02/27/95
02/28/95
AVG:
MAX:
MIN:
FLOW:
cm
2324
2909
467
1761
2037
1800
1965
888
1172
2197
2243
1895
2011
2034
1949
1034
1714
1652
2173
2237
1940
2187
1914
2314
2196
2026
2767
2572
1942
2909
467
PH:
pH
5.2
5.1
5.3
5.4
5.3
5.4
5.4
5.4
5.4
5.4
5.5
5.4
5.3
5.3
5.2
5.1
5.0
5.0
5.1
5.3
5.3
5.3
5. 1
5.2
5.2
5.3
5.2
5.2
5
6
5
-
FEB.WK1
=,
ppm
7280
10460
6760
6810
6760
8180
7860
7880
7390
11360
6700
7040
6000
7300
9310
9140
6910
5530
6150
6710
6400
6250
6100
6560
6650
6100
4050
6170
7136
11360
4050
Page 1 of 10
-
#21TC1
iSS:
ppm
4
10
11
9
10
10
13
9
13
36
21
18
11
9
9
7
18
16
10
7
11
6
7
6
36
17
7
28
13
36
4
-
TOG:
ppm
1407
3306
1413
2927
2263
3306
1407
- -- -- - - -
FEB.WK1
GAOLN)WATER MONTH..Y MONITOAlNG:
OUTER TIER COMBINED t-FLUENT:
PAGEN0.1
FEB.1995
DATE:
02/01/95
02/02/95
02/03185
02/04/95
02/05/95
02106/95
02/07/95
02/08/95
02/09/95
02/10/95
02/11/95
02/12/95
02/13/95
02/14/95
02/15195
02/16/95
02/17/95
02/18/95
02/19195
02/20/95
02/21/95
02/22/95
02/23/95
02/24/95
02/25195
02/26/95
02/27/95
02/28/95
AVG:
MAX:
MIN:
FLOW:
cm
83545
85148
76353
87683
87825
87103
87764
86609
87273
87427
85001
86690
87130
88120
86324
88070
86485
84146
85248
66444
83996
65932
86964
79596
68471
80946
70414
84841
82841
88070
65932
PH:
pH
5.6
5.4
5.5
5.4
5.2
5.5
5.7
5.8
5.8
5.4
5.7
5.7
5.5
5.6
5.5
5.4
5.3
5.4
5.3
5.5
5.5
5.4
5.5
5.4
5.4
5.4
5.3
5.5
5
6
5
TOC:
ppm'
4.6
26.9
9.9
15.8
14
27
5
#1 OTCI
Page 2 ol 10
- -- -
---
GROUNDWATER MONTl-L Y MONfTOAN'.3:
SBA MIXED LIQUOR:
PAGE N0.4
FEB.1995
DATE:
02/01/95
02/02/95
02/03/95
02/04195
02/05/95
02/06/95
02/07/95
02/08/95
02/09/95
02/10/95
02/11/95
02/12/95
02/13/95
02/14/95
02/15195
02/16/95
02/17/95
02/18/95
02/19/95
02/20/95
02/21/95
02/22/95
02/23/95
02/24/95
02/25/95
02/26/95
02/27/95
02/28/95
AVG:
MAX:
MIN:
PH
pH
8.2
7.9
6.2
8.1
8.0
8.1
8.1
8.2
8.1
8.1
8.1
8.1
8.0
8.1
8.0
7.9
8.0
8.1
8.2
8.1
8.1
8.1
8.0
8.1
8.0
7.9
8.0
8.1
8
8
6
S131J.1L
NH3N: P04:
ppm Pflrn
112 15.0
135 18.0
132 16.5
140 17.0
134 16.4
130 33.5
197 32.4
117 29.2
159 27.8
114 25.4
99 21.4
115 22.0
130 22.8
133 20.6·
100 8.6
154 16.6
123 32.4
126 31.4
132 33.0
139 8.4
137 12.0
128 23.9
135 16.3
143 14.9
135 16.0
1 29 12.0
110 13.9
137 21.7
131 21
197 34
99 8
DO:
ppm
2.0
3.9
3.2
2.9
2.8
2.9
2.6
2.6
2.8
2.7
2.5
3.0
2.2
3.0
3.0
1.2
2.1
2.2
1.9
3.7
2.4
2.2
1.5
2.0
3.0
2.9
2.7
3.2
3
4
- ---
FEB.WK1
SETT. SLLOGE
MLSS: MLVSS: SOLOS:WASTE[F/M:
ppm ppm ml/1 gal ratio
2040 1536 80 344 0.24
1560 75 108 0.35
1760 65 81 0.00
1920 65 54 0.29
2000 65 54 0.31
1764 70 45 0.41
1504 70 54 0.43
1516 960 70 40 0.38
1652 75 40 0.39
1480 80 45 0.39
1616 80 54 0.39
1800 85 60 0.32
1-4 76 85 97 0.36
1636 90 45 0.33
2000 1500 90 40 0.31
2124 95 40 0.26
2240 80 51 0.21
2120 95 40 0.27
2000 96 40 0.25
1904 85 45 0.26
1960 90 40 0.26
2124 1540 90 50 0.27
2752 90 50 0.17
2452 85 62 0.19
2312 90 40 0.25
2252 100 54 0.24
2604 100 54 0.18
2768 100 67 0.16
1976 1384 84 64 0
2768 1540 100 344 0
1476 960 65 40 0
Pege 3 of 10
5/DAY
F/M:
ratio
0.18
0.24
0.27
0.29
0.36
0.38
0.40
0.39
0.37
0.37
0.36
0.34
0.32
0.29
0.28
0.26
0.25
0.25
0.26
0.24
0.23
0.23
0.22
0.21
0.20
0
0
0
-- - ----
GROLN)WATEA MONTH. Y MONITORING:
AFTER Pl.ATE SEPARATOR BEFORE SBA:
PAGEN0.3
FEB.1995
DATE:
02/01/95
02/02/95
02/03/95
02/04/95
0 2105/9 5
0 2/06/95
02/07/95
02/08/95
02/09195
02/10/95
02/11/95
02/12/95
02/13/95
02/14/95
02115/95
0 2116/95
02/17/95
02/18/95
02/19/95
02/20/95
02/21/95
02/22/95
02/23/95
02/24195
02/25/95
02/26/95
02/27/95
02/28/95
AVG:
MAX:
MN:
PH:
pH
5.2
5.5
6.2
6.1
5.8
5.8
5.6
6.7
6.0
5.8
5.8
5,6
5.8
8.3
5.6
8.4
8.1
5.7
5.9
5.8
5.5
6.1
5.8
5.8
5.8
5.8
5.5
6
7
5
COO:
ppm
5610
6090
6360
6880
8150
7200
6520
7170
6430
7000
6500
5950
6070
6990
6270
5210
6350
5730
5530
5700
6560
5340
5210
6500
6000
5350
4950
6208
8150
4950
FEB.WK1
TSS:
ppm
40
44
40
48
40
32
44
40
44
28
28
24
44
40
44
40
36
44
40
28
40
44
40
24
20
44
24
37
48
20
Pege 4 of 10
--- -
=
------
FEB.WK1
GRCXJNDWATEA MONTH.. Y MONrTORl(',_K3:
SBA EFFLUENT:(DECANT) #4 SBAE
PAGEM:l5
FEB.1995 WAS. NH3N
DATE: FLOW: COil TSS:TSS ADOEU:
CfU ppm ppm ppm gal
02/01 /95 2058 849 120 8640 2
02/02/95 2229 907 236 24440
02/03/95 816 120 9600
02/04/95 2000 809 112 12200
02/05/95 1980 769 120 12000 2
02106/95 2219 765 96 10620
02107/95 1965 678 244 13720
02/08195 1863 620 200 16400
02/09/95 1891 605 247 17800
02/10/95 1983 570 128 11740
02/11/95 1900 555 140 11220 3
02/12/95 1955 540 180 11620 2
02/13/95 1698 495 178 13620
02/14/95 2189 486 158 12640
02115/95 2026 469 128 13940 3
02/16/95 790 442 124 12600
02/17/95 2228 423 160 13600 1
02/18195 2313 404 140 13800 2
02/19/95 2305 343 124 13800 2
02/20195 2402 310 120 13920
02/21/95 2307 290 164 13500
02/22/95 2311 315 160 15800
02/23195 2291 270 120 17100
02/24/95 2327 255 114 16400 1
02/25/95 2288 275 1<0 14880 2
02/26/95 2276 245 180 13800 3
02/27/95 2297 226 132 15900
02/28/95 2330 231 68 14820
AVG: 2097 498 149 13933
MAX: 2402 907 247 24440 3
MIN: 790 228 88 8640
DO NOT PACCESS SBR
Pe.ge 5 of 10
-
PHO&
ADDED:
lbs
3
2
2
1
2
2
3
2
1
3
3
1
2
2
2
3
3
2
3
---- ----
FEB.WK1
GAOl.N)WATER MONTH.. Y MONITORING:
INNER TIER EQUALIZATION TANK: !TECT
PAGE NO.?.
FEB.1995
DATE: PH: COO: OT WATER ADDED
02/01/95
02/02/95
0 2/0 3/9 5
02/04/95
02/05/95
02/06/95
02/07/95
02/06/95
02/09/95
02/10/95
02/11195
02/12/95
02/13195
02114195
02/15/95
02/16/95
02/17/95
02/18/95
02/19/95
02/20/95
02/21195
02/22/95
02/23/95
02124/95
02125/95
02/26/95
02/27/95
02/28/95
AVG:
MAX:
MN:
pH
7.8
7.4
7.6
7.7
7.8
8.5
8.6
8.8
8.9
8.9
7.9
7.8
8.0
6.7
8.5
8.7
6.8
6.9
7.0
6.6
6.7
6.7
6.8
6.9
6.8
6.8
6.9
8.8
7
9
7
ppm
6780
8790
5970
6210
6470
6740
8920
8810
7530
7880
6400
6300
5900
6360
7120
5180
5650
6240
5610
5220
5650
6300
4670
5560
6300
5600
5050
4940
6363
8920
4670
gal
450
450
450
450
Pe.ge 6 or 10
--
---- - -
FEB.WK1
GROUNDWATER Mctm-1. Y MONITOR~:
INNERTIER CARBON FLTER EFFLUENT
PAGE NO. 7 #8 ITEF
FEB.1995
DATE:
02/01195
0 2/0 2/9 5
0 2/0 3/9 5
02/04/95
02/05/95
02/06/95
02/07/95
02/08/95
02/09/95
02/10/95
02/11/95
02/12/95
02/13/95
02/14/95
02/15/95
02/16/95
02/17195
02/18/95
02/19/95
02/20/95
02/21/95
02/22/95
02/23/95
02/24/95
02/25/95
02/26/95
02/27/95
02/28/95
AVG:
MAX:
MIN:
PH:
pH
8.1
8.2
8.2
8.1
8
8
8
COD:
ppm
808
595
448
295
537
606
295
TOC:
ppm
71
152
101
48
81
152
35
TSS:
ppm
35
35
35
35
Page 7 of 10
-- -- - --- -
GAOLIDWATER MONTH.. Y MONTTOAIOO:
ourER TIER CARBCN FL TEA EFFLUENT:
PAGEN0.3
FE:8.1995
DATE:
02/01/95
02/02/95
0 2/03195
02/04/95
02/05/95
O 2/06/95
02/07/95
02/08/95
02/09/95
02/10/95
02/11/95
02/12/95
02/13/95
02/14/95
02/15/95
02/16/95
02/17/95
02/18/95
02/19195
O 2/20/95
02/21195
02/22/95
02/23/95
02/24/95
02/25/95
02/26/95
02/27/95
02/28/95
AVG:
MAX:
MIN:
PH:
pH
7.2
6.9
6.9
6.5
7
7
7
TOC:
ppm
4.0
14.0
27.4
11.9
14
27
4
TSS:
ppm
4
4
4
4
FE8.WK1
Page 8 of 10
- ---
#7 OTEF
---- - --- - -
FEB.WK1
GROUNDWATER MCNTH...Y MONITOR~:
RAINFALL DATA
DATE CHESl()AY
02/01/95 0.00
02/02/95 0.00
02/03/95 0.00
02/04/95 0.00
02/05/95 0.00
02/06/95 0.00
02/07/95 0.00
02/08/95 0.00
02/09/95 0.00
02/10/95 0.30
02/11 /95 0.00
02/12/95 0.00
02/13/95 0.00
02/14/95 0.40
02/15/95 1.50
02/16/95 1.90
02/17/95 0.50
02/18/95 0.10
02/19/95 0.00
02/20/95 0.00
02/21/95 0.00
02/22/95 0.00
02/23/95 0.10
02/24/95 0.00
02/25/95 0.00
02/26/95 0.00
02/27/95 0.80
02/28/95 0.40
TOTAL 5.90
AVG 0.74
Page 9 of 10
- ---
GROUNDWATER TREATMENT PLANT
( 1) INNERTIERSYSlEM
FEB.1995
ITEM INFLUENT EFFLLENT
-------------------
FLOW -TGD 1.9 1.9
-- --
FEB.WK1
%RED. N'.JTES
02/16/95 LIGHTNING TRIPPED
BLOWER OFF.NO 00 READING AT
0700 HRS. MIXER TURNED ON BY
COD -mg/l 7136 537 92.5% ACCOENTWHLE DECANTING FROM
TSS
pH
mgll 13.2 37.2
LOW 5.0 8.1
HIGH 5.5 8.2
GROLNJWATER TREATMEITT Pl.ANT
(2) OUTERTEASYSTEM
ITEM lr-.FLU:NT EFFLLENT % RED.
FLOW • TGD
TSS
pH
mg/L
LOW
HIGH
82.8
5.2
5.8
82.8
4.0
6,5
7.2
Page 10 of 10
SBA.STOPPED DECANTING 755
GALS PRCCESSED.
-
, - --- --- -- - ------ -- -
FEBREF.WK1
OAI\.Y FEFEReCE SHEET:
OATE: ff, £0 PLT. DEC. DEC. w.s "" "' "' "' MS "' "" "" ""· TNK SEP. LIO LJ(l LJ(l AOO ADO LIO WAS s,o.-.v
1111'15 COO, coo coo. COO. = = """' "' MS ""' LBS SCT, c,,t!: rn,; AVG.
7280 ~!!~ !,(;l,j "' 120 8840 2040 '" 15.0 80 , .. 0.24
1041!10 11790 8090 '" "' 2,Ho 1 580 '" 18.0 " '" 0.35
871!10 5970 '" 120 11800 \JeO '" Hl.5 " " 6810 11210 8380 "' '12 1 2200 1920 '" 17.0 " " 0.211
8780 U70 &&110 "' '20 1 2000 2000 ,,. 18.4 " " 0.31 0.2,
8180 11740 11150 "' " 1 01120 1784 '" 33.S TO " o . .i 0.27
7880 81120 7200 "' , .. 1 3720 1504 "' 32.4 TO ,. o.u 0.211
78110 6810 6520 "' ,oo 11'400 , 51 e '" 29.2 TO " 0,38 0.38
7390 7530 7170 805 "' 17800 11152 "' 27.1 75 " 0.311 0.38
" 11380 71180 8430 "' '" !\HO 1'80 ',. 25.4 " " 0.39 0.40
" 1'700 8400 1000 555 '" 11220 1111 II " 21., " ,. O,Jll 0.311
" 7040 8300 8500 "' '80 111520 1800 '" 22.0 85 " 0.32 0.37
" 8000 51100 5950 "' '" 1 3820 \"78 '" 22.11 " ., 0.38 0.37 ,. 7300 8380 8070 ... '" 1 21140 18311 "' 20.8 " " 0.33 0.311
" 1131 0 71 20 1111110 "' "' 13940 2000 ,oo •• " " 0.31 0.3,
" 111'0 5180 11270 .., ,,. 1 2&00 212, '" 111.11 .. " 0.211 0.32
" 1101 0 51150 521 0 "' '" 1 3eoo 2240 "' 32., 80 " 0.21 0.20
" 5530 11240 e351l '" '" 13800 2120 "' 31.4 .. " 0.27 0.211
" II 1 !!iO 5e1 o 51130 '" ,,. 1300 2000 '" 33.0 .. " 0.25 o.2e
" 11710 &220 5530 '" "o 131120 11104 '" , .. " " 0.211 o.:a
" 11,00 lillliO &700 "' '" 13500 111110 "' 12.0 00 " 0.211 0.25
" 11250 eJoo 115fl0 ". '" 151100 212, '" 23.0 00 50 0.21 0.211
" 11100 ,1110 5340 m '" 17100 2752 "' 111.3 00 50 0.1 7 0.24 ,. 115110 55110 521 0 "' '" 111400 2452 '" 14.0 " " 0. 1 0 0.23
" 111150 11300 11500 m '" 1411eo 2312 '" HI.O 00 " 0.25 0.23
" II 1 00 51100 8000 "' '" 131100 2252 "' 12.0 ' ' ,oo " 0.2, 0.22
" 4050 5050 5350 "' '" 15900 2804 '" 13.0 ' '00 " 0.111 0.21
" 11170 ,o,o 4050 "' " 1 ,1120 27118 "' 21.7 '00 " 0. I II 0.20
AVG· 71311 &nJ 11205 "' "' 130311 19711 '" 20.7 .. .. 0.211
""" 113110 11020 111 50 "' "' 2u40 27118 "' 33.!!i ,oo , .. 0,43
MN· 4050 41170 4050 "' " 8UO 1'711 " •• " " 0.111
NOTE
010 NOT PROCESS OZOMl!!i OE CANT COO HlGH.
i
-
MARCH
1995: IT-1
03/01/95 206
03/02/95 219
03/03/95 226
03/04/QS 223
03/05/95 228
03/06/95 211
03/07195 208
03/08195 231
03/09195 224
03/1 0/95 228
03111/95 231
03112/95 228
03113/95 241
03114/95 194
03/16/115 183
03118/95 198
03/17/95 193
03/18/95 193
03119/95 177
03/20/95 183
03/21/95 210
03/22195 196
03/23/95 199
03/24195 197
03/25/95 I 94
03/26/95 194
03/27195 248
03/28/95 199
03/29/95 241
03/30/95 253
03/31/95 253
AVG:
TOT:
213
6605
-
IT•2
6B
72
68
67
55
58
57
47
47
47
54
52
51
48
63
54
51
53
70
80
87
80
50
43
34
31
79
64
78
75
81
58
1794
-
IT-3
269
195
229
242
270
255
211
337
210
182
193
200
201
192
188
200
208
202
193
183
187
185
190
193
189
198
188
149
192
180
191
206
--
IT-4
190
186
177
179
195
362
294
467
251
246
294
290
285
230
218
215
231
267
259
221
192
213
261
285
288
255
223
178
195
182
184
242
WELLS.WKl
NIJERTIEA
DAILY FLOW:
IT-5
216
373
299
347
333
328
363
273
200
272
361
443
358
304
304
351
396
375
361
291
281
278
279
276
253
299
281
248
287
277
305
310
IT-6
140
119
21
97
135
213
227
207
224
226
244
246
243
219
209
225
246
242
225
205
212
212
225
245
237
241
240
186
213
210
234
205
6398 7495 9610 4337
-
IT-7
196
195
203
212
212
197
201
136
112
115
227
230
229
197
196
208
224
212
192
192
202
194
200
216
214
217
208
168
192
2
417
197
6116
-
IT-8
227
229
233
259
265
51
317
343
367
18
14
34
301
268
239
244
274
265
254
241
252
247
250
288
283
32
0
12
0
270
353
208
6450
-
IT-9
1059
1066
1100
1146
1135
10B2
1135
1046
1079
1119
1222
1220
1208
10Q7
1032
4
976
1251
1152
1065
1083
1097
9
1110
1223
325
3
974
1134
105
3
912
28260
2551
-- -
M'.RCH
1QQ5: OT-I OT-2
03/0 1 IQ5 20600 23177
03/02/QS 21100 231Q8
03/03/Q5 21800 237Q4
03/04/Q5 20100 22512
03/05/Q5 21200 23991
03/06/Q5 21200 24052
03/07/95 21300 24326
03/08/95 21100 24522
03/09/Q5 21000 23777
03/10/Q5 18700 22575
03/11/Q5 21900 22884
03l 12/Q5 22300 22946
03113/95 22100 23450
03/14/95 24600 26768
03/16/95 22000 25352
03116/QS 1Q400 27853
03/17/95 21900 246QQ
03/18/95 22000 24872
03/19/95 19300 21795
03/20/95 20300 22865
03/21/95 22200 25348
03/22/95 21900 25326
03/23/95 22200 25925
03/24195 21900 25541
03/25/96 21900 24622
03126/95 22500 25677
03/27/Q5 22000 24Q26
03/28/95 22100 24951
03/29/Q5 20300 23141
03/30/95 11200 28201
03/31195 22200 24974
AVG: 21100 24453
- -- -
WELLS.WK1
OJTERTIER
DAILY FLOW:
OT-3 OT-4 OT-5 OT-6
2011 1237 2281 6916
2074 1258 2322 6971
2056 1283 2339 7028
2022 1219 2151 6516
2137 1275 2246 6812
2137 1263 2230 6738
2160 1269 2208 6809
2090 1259 2168 6765
2086 1252 1876 6705
2031 1237 2026 6482
2150 1267 2057 6735
2165 1281 2085 8775
2149 1269 2249 8781
2060 1287 2829 8823
2108 1290 2595 6742
2152 1323 2992 6889
2149 1317 2017 6725
2153 1342 2236 8737
2174 1359 1683 6108
2143 1354 2413 6316
2178 1377 2845 6878
2150 1369 2592 6794
2175 1387 2495 6888
2132 351 2218 6753
2138 2358 2283 6758
2208 1397 2305 6985
2140 1353 1821 6782
2152 1368 1893 6814
2175 1401 1979 6368
1792 1374 2615 6602
2186
2117
1401 2630 6916
1315 2272 6738
OT-BA OT-7 '--
7140 2512
7294 2567
7406 2624
6800 2444
7061 2568
6994 2552
6961 2561
6960 2549
6888 2531
6522 2418
6586 2505
6822 2522
6597 2497
7860 2557
6770 2511
7025 25 77
6551 2525
6497 2534
5752 2282
5966 2360
6522 2552
6453 2513
6531 2550
6397 2524
6402 2518
8590 2603
6387 2523
6397 2528
5902 2350
6503 2404
6535
6667
2535
2510
TOT: 854100 758040 85629 40787 70437 208891 206671 77796
-
17700
17900
18300
17000
18200
18200
18500
18900
18800
18600
19200
19800
18900
0
19800
20800
19300
19200
17100
17700
19300
19000
19300
19000
18900
19500
19000
18900
17500
18900
18900
18126
6E+05
85298
-
-- ------.. - - -- ---
ITMAINT1.WK1
MAINTENANCE ACT1VITIE&-GROl.R'.JDWATER OPERABLE UNIT #1
INf'.ERTER SYSTEM
ACTION
DATE LOCATION PROOIEM DATE ACTION MEC!W-IC
03/03/95 IT-6 LO',VFLOW 03/03/95 REPl.J\CED EXHAUST OONTROL PP JP
VALVE
03/13/95 IT-1 LOW FLOW 03/13/95 ADJUSTED EXHAUST VALVE & JPPP
Th<ER
03/13/95 IT-7 LOW FLOW 03/13/95 REPAIRED BUBBLER n.JBE PPJP
03/13/95 IT-8 LOW FLOW 03/13/95 RESET & a...EANED SCREEN PPJP
03/13/95 IT-5 LOW FLOW 03/13/95 REPlACED
BLADDER.ADJUSTED FLOW
CLEA/'JEO SCREEN
JPPP
03/14/95 SBRBLONEA AIR LEAK 03/14/95 REPLACED BALL VAL VE JPPP
EXHAUST VALVE
a:ffifUER
03/20/95 IT-1 LOW FLOW 03/20/95 SETFLOW JPPP
03/27/95 IT-1 LOWA.OW 03/27/95 ctENED STFWt-ER PPJP
03/27/95 IT-2 LOW FLOW 03/27195 Cl.ENE□ STRAlt-EA
REPlACED BIADDER JPPP
03/27/95 IT-5 LOW FLOW 03/27/95 Cl£Ar-ED STRAlt-ER
REPLACED BL.ADDER JPPP
03/28/95 IT-8 LOW FLOW 03/28/95 RESET CONTACX..S
ClEAt-ED STRAIM:A JPPP
03/28/95 IT-9 LOW FLOW 03/28/95 RESET CCNTACX_S JPPP
03/30195 IT-8 LOW FLOW 03/30/95 RESET CONTRCl..S JPPP
Page 1 of 1
------..
OTMAINT1.WK1
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
WTERTERSYSTEM
ACTION
DATE LOCATION PFal.EM DATE ACTION
03/03/95 OT-1 LOW Fl.OW 03il3/95 CLEAM:D STRAlt-ER
031131gs OT-5 LOW FLOW 03/13/95 ADJUSTED FLOW
03/20/95 OT-5 LOW FLOW 03/20/95 SETFlOW
03/20/95 OT-SA LOW FLOW 03/20/95 SETFlOW
03/29/95 OT-5 LOW FLOW 03/29/95 SET FLOW
CLENED STRAlt-ER
--
MEG--W-ik..:
.PPP
.PPP
.PPP
.PPP
.PPP
03/29/95 OT-7A LEAK 03/29/95 Pllk3GEO LtE TO Pl.J.4P .PPP
Page 1 of 1
--------
-----------...
RAINFALL.WK1
GROUNDWATER MONTH.. Y MONITORING:
RAINFALL DATA
O,.,TE INCi-ES/DAY
03/01/95 0.00
03/02/95 0.00
03/03/95 0.25
03/04/95 0.00
03/05/95 0.40
03/06/95 0,00
03/07/95 0.00
03/08/95 0.60
03/09/95 0.00
03/10/95 0,00
03/11/95 0.00
03/12/95 0.00
03/13/95 0.00
03/14/95 0.00
03/15/95 0.00
03/16/95 0.00
03/17/95 0.00
03/18/95 0.00
03/19/95 0.00
03/20/BS 0.50
03/21/95 0.00
03/22/95 0.00
03/23/95 0.00
03/24/95 0.00
03/25/95 0.00
03/26/95 0.00
03/27195 0.00
03/28/95 0.00
03/29/95 0.00
03/30/95 0.00
03/31/95 0.00
TOTAL 1.75
AVG 0.44
Page 1 of 1
-- ----... -----...
MAR.WK1 MAR.WK1
GRCUNOWATEAMONTHLYMONJTOAING: GAOltOWATER~YMONITOAll'Ki:
INNER TIER COMB NED NFLUENT #2 ITCI OUTER TEA COMBtEO IM1.UENT: #1 OTCI
PAGE00.1 PAGEN0.1
MAR. 1995 MAH.1995
DATE: FLOW: PH: CCX); TSS: TOG: DATE: FLOW: PH: TOG:
GD pH ppm ppm ppm cro pH ppm
03/01 /95 2338 6.4 5050 10 03/01/95 83554 5. 7
0~/02i95 2176 5.4 5650 11 1712 03/02/95 84684 5.7 38.8
03/03/95 2278 5.5 5500 7 03/03/95 86430 5. 7
03/04195 2362 5.4 5195 9 03/04/95 80764 5.6
03/05/95 2261 5.3 6710 10 03/05/95 85490 5.5
03/06/95 2207 5.4 61 70 1 0 03/06/95 85366 5.8
03/07'95 2455 5.4 6740 1 0 03/07/95 86094 5. 7
03/08/95 2338 5.4 6050 9 1 794 03/08/95 86313 5.6 4.1
03/09/95 2734 5.6 4920 7 03/09/95 84915 5.8
03/10/95 1872 5. 7 6250 10 03/10/95 80591 5.7
03/11/95 2153 5.4 6850 14 03/11/95 85254 5.6
03/12/95 2208 5.4 7200 11 03/12/95 85576 5. 7
03/13/95 3115 5.4 7130 14 03/13/95 85972 5.6
03/14/95 2749 5.5 6260 10 03/14/95 74604 5.6
03115195 2620 5.4 6210 10 03/15/95 66968 5.6
03/16195 1699 5.4 5560 10 2006 0 3/1 6/95 91011 5. 7 9.2
03/1 7195 2115 5.4 8010 25 03/17/95 87183 5.7
03/18/95 2604 5.4 6780 12 03/18/95 87571 5.6
03/19/95 2883 5.5 6650 10 03/19/95 77533 5.5
03/20/95 2641 5.4 6520 1 0 03/20/95 81418 5.6
03/21 /95 2686 5.4 7150 6 03/21/95 88998 5.8
03/22/95 2682 5.4 6150 6 03/22195 88097 5.6
03/23/95 1663 5.4 6700 11 2114 03/23/95 89451 5.7 5.6
03/24/95 2338 5.3 7700 51 03/24/95 86814 5.7
03/25/95 2407 5.4 6800 15 03/25195 87877 5.6
03/26/95 1790 5.4 6550 21 03/28/95 89763 5.6
03/27/95 1468 5.3 12370 40 03/27/95 86934 5.6
03/28/95 1884 5.2 121 70 60 03/28195 87103 5.8
03/29/95 2532 5.5 6440 6 03/29/95 81116 5.7
03130/95 1554 5.4 6590 6 1999 03/30/95 79591 5.7 7.0
03131 /95 14 79 5.3 8970 17 03/31 /95 88277 5.7
AVG: 2267 5 6871 1 5 1925 AVG: 85268 6 13
MAX: 3115 6 12370 60 2114 MAX: 91011 6 39
MIN: 1468 5 4920 6 1712 MN: 74604 6 4
Page 1 ol 10 Page 2 of 10
--------------------------.. -.. .. ---.. -...
MAR.WK1 MAR.WK1
GROUNOWA TEA MONlH.. Y MONrTCflNG: GAOLN)WATEA MONTI-LY MONITORING:
SBA MIXED lk)ll()R: SffiM_ AFTER Pl.ATE SEP Ar.ATOR EEFORE SBA:
PAGE NO. 4 PAGEN0.3
MAA.1995 SETT. S..t!JCE 5/DAY MAA.1995
DATE: PH NH3N: P04: DO: UI""' ,........,,.,. M..VSS: SOLOS: WASTED F/M: F/M: DATE: PH COO: TSS:
pH ppm ppm ppm ppm ppm ml/I gal re!lo ratio pH ppm ppm
03/01/95 8.2 115 11.8 3.2 24 76 1600 85 57 0.18 03/01/95 6.0 4910 28 -,I
03/02/95 8.2 111 16.6 3.5 2296 \00 67 0.22 03/02/95 5.6 5800 20
03/03/95 8.2 125 22.8 3.3 2416 100 57 0.17 03/03/95 5.8 4490 38
03/04/95 8. 1 130 24.0 2.5 2440 80 5' 0.23 0.16 03/04/95 6. 1 6410 40
03/05/95 8.0 134 25.0 2. 1 2448 100 65 0.22 0.20 03/05/95 6.2 6090 48
03/06/95 8. 1 93 13.7 2.4 2600 120 62 0.21 0.21 03/06/95 5.8 6090 24
03/07/95 8. 1 134 10.6 3.3 2520 1\ 0 54 0.21 0.21 03/07/95 5.5 5860 28
03/08/95 8. 1 112 25.3 3. 7 2628 1852 110 94 0.15 0.20 03/08/95 5.5 4540 40
03/09/95 8.3 120 16.2 2.9 2416 100 65 0.21 0.20 03/09/95 5. 7 5770 32
03/10/95 8.2 116 13.8 3.0 3004 130 8\ 0.16 0.19 03/1 0/95 7.1 5410 36
03/11 /95 8. 1 1\ 9 14.4 3.1 2516 135 75 0.22 0.19 03111 /95 5.8 6100 28
03/1 2/95 8.0 132 20.0 3.8 2364 115 8\ 0.24 0.20 03112/95 5.8 6250 20
03/13/95 8. 1 136 10.3 3.2 2728 110 73 0.22 0.21 03113/95 6.7 6730 28
03/14/95 8.0 140 30.1 3. 1 1872 11 0 \05 0.28 0.22 03/14/95 6.3 5896 20
03115/95 7.8 130 17.0 1.7 2920 1640 115 61 0.17 0.22 03/15/95 8.4 5710 38
03/16/95 8.0 138 12.2 1.7 2600 115 78 0.20 0.22 03/18/95 5.8 6160 46
03/17/95 7.9 128 17.0 1.5 2784 120 63 0.20 0.21 03/17/95 5.4 6360 40
03/18/95 7.6 130 20.0 1 .5 2600 120 100 0.25 0.22 03/18/95 5.8 7900 40
03/19/95 7.8 125 19.0 \.8 2640 125 \35 0.18 0.20 03/19/95 5.7 5810 36
03/20195 8.0 154 12.6 \.2 2844 \30 87 0.19 0.20 03/20/95 5.5 6140 32
03/21195 7.8 182 22.7 0.1 3340 125 100 0.16 0.20 03/21/95 8.3 6160 40
03/22/95 6.3 159 21.0 1.7 2888 1680 125 95 0.18 0.19 03/22/95 5.4 5800 16
03/23/95 8.0 148 7.9 0.4 3088 1\ 5 105 0.18 0.18 03/23/95 5.8 6170 18
03/24/95 8.0 166 15.3 2.4 3020 \30 108 0.17 0.18 03/24/95 5.7 5800 20
03/25/95 7.9 156 16.0 2.5 2796 125 100 0.20 0.18 03/25/95' 6.1 6200 24
03/26/95 6.0 154 19.3 2.7 2724 125 108 0.21 0.19 03/26/95 7.8 6500 26
03/27/95 7.9 144 9.9 1.7 3146 \30 97 0.19 0.19 03/27/95 5.7 6550 48
03/28/95 7.7 155 17.8 \.9 3480 125 62 0.00 0.15 03/28/95
03/29/95 7.9 186-20.6 1.5 3364 1644 120 \08 0.22 0.16 03/29/95 5.3 8430 28
03/30/95 8. 1 166 23.9 0.9 3160 120 100 0.19 0.16 03/30/95 8.0 6780 48
03/31 /95 8.0 153 9.0 \.3 5400 130 100 0.06 0.13 03/31 /95 6.5 3890 40
AVG: 8 138 17 2 2843 1683 11 7 85 0.19 0 AVG: 6 6024 32
MAX: 8 186 30 4 5400 1852 \35 \35 0.28 0 MAX: 8 8430 48
MIN: 6 93 8 0 1872 1600 80 54 0.00 0 Mt.I: 5 3890 1 6
.
Page 3 of 10 Page 4 of 10
-------.. .. -... 111111 ----...
MAA.WK1 MAR.WK1
GROUOOWATEA t.10NTl-L Y MONrTOOJN'.3: GROlN)WATEA MONTH.. Y MONITOA.00:
SBA EFFLUENT:(OECANTI #4 SBRE INNER TIER EQUALIZATION TA.Nit:: ITEOT
PAGEN0.5 FAGl:::.N0.2
MAR.1995 WAS. NH3N PHO& MAR.1995
DATE: FLOW: 000: TSS: lSS ADDED: ADDED: DATE: PH: CCO: OT WATER ADDED
cro ppm ppITT ppm gal lbs pH ppm gal
03/01195 2339 226 144 12640 3 03/01/95 6.7 6050
03/02/95 2239 235 112 11900 2 3 03/02/95 6.9 5700
03/03/95 2163 237 120 13460 03/03/95 7.0 5950
03/04/95 2325 246 112 13600 1 03/04/95 7.1 6160
03/05/95 2253 231 116 12400 1 03/05/95 7.2 5960
03/06/95 2319 207 104 12840 3 3 03/06/95 6.9 6220
03/07/95 2345 1 •• 56 15760 3 03/07/95 6.9 6310
03/08/95 2394 140 72 15080 1 03/08/95 7.0 4640
03/09/95 2308 130 40 14440 1 2 03/09/95 7.2 4970
03/1 0195 2252 120 BO 15300 2 3 03/10/95 7.1 5520
03/11195 2276 135 104 14140 2 3 03/11195 7.0 6000
03/1 2/95 2244 145 64 13860 1 1 03/12/95 ••• 6300 (
03/13/95 2316 135 24 17180 2 3 03/13195 7.0 7100
03/14/95 2318 110 32 17220 1 03/14/95 7.8 6320
03/15/95 2269 106 48 18840 2 2 03/15/95 7.0 5760
03/16/95 2310 150 56 15660 2 2 03/16/95 6.9 4950
03/17/95 2313 175 40 17760 3 3 03/17/95 7.1 8100
0311 B/95 2184 135 64 17400 3 3 03/18/95 7.0 8250
03/19/95 2215 175 96 17200 2 03/19/95 7.2 6730
03/20/95 2238 190 60 15480 2 2 03/20/95 7.1 6360
03121 /95 2246 160 86 1 7780 03121/95 7.0 7445
03/22/95 2243 176 •• 17040 03/22/95 6.8 6000
03/23/95 2274 165 44 15200 3 3 03/23/95 7.0 6070
03/24/95 2257 165 64 15220 03/24/95 6.8 6000
03/25/95 2173 150 86 15680 3 03125/95 6.8 6400
03/26/95 2284 160 120 14980 3 03/26/95 6.7 6350
03/27/95 2311 160 100 16600 3 3 03/27/95 7.1 7560 25.0
03/28195 15600 03/28/95 7.1 9250 1 8,0
03/29/95 2092 190 52 17120 2 2 03/29/95 7.2 7560
03/30/95 2232 305 106 17160 03/30/95 6.9 6950
03/31195 2205 165 72 16800 0 3 03/31195 6.9 7430
AVG: 2265 174 81 15527 2 2 #DIV/01 AVG: 7 6464 22
MAX: 2394 305 144 18840 3 3 0 MAX: 8 9250 25
MN: 2092 106 24 11900 0 0 MN: 7 4640 18
Page 5 or 10 Page 6 ol 10
- ------.. -.. ----.. -
MAA.WK1 MAA.WK1
GRCX.Jt,OWATER MONH--l.. Y MONITOON3:. GAa.JOOWATEA MONTHLY MONITOAIN3:
HER TEA CAR0CN FL 1ffi EFFLUENT #8 ITEFITEACNUJONFLTEREFFLU:.NT: #7 OTEF
PAGE NO. 7 PAGEN0.3
MAA.1995 MAA,19U5
DATE: PH: COO: toe: TSS: DATE: PH: TOC: TSS:
pH ppm ppm ppm pH ppm ppm
03/01 /95 7.1 215 30 03/01/95 6.9 4.0 l 03/02/95 59.1 03/02/95 17.4
03/03195 03/03/95
03/04/95 03/0-4/95
03/05/95 03/05/95
03/06/95 03/06/95
03/07/95 03/07195
03/08/95 B.3 130 43.9 03/08/95 6.9 3.7
03109/95 03/09/95
03/10/95 03/10/95
03/11 /95 03111 /95
03/12/95 03/12/95
03/13/95 03/13/95
03/14/95 03/14/95
03/15195 8.3 128 03115/95 7.0
03/16/95 39.8 03/16/95 4.2
03/17195 03/17/95
03/18/95 03/18/95
03/19/95 03/19195
03/20/95 03/20/95
03/21 /95 03/21 /95
03/22/95 B.2 150 03/22/95 6.9
03/23/95 26.5 03/23/95 3.9
03/24/95 03/24/95
03/25/85 03/25/95
03/28/95 03/26/95
03/27/95 03/27/95
03/28/95 03/28/95
03/29/95 ,., 174 03/29/95 8.8
03/30/95 30.4 03/30/95 3.7
03/31 /95 03/31/95
AVG: ' 159 40 30 AVG: 7 7 4
MAX: ' 215 59 30 MAX: 7 " 4
MN: 7 126 27 30 MN: 7 4 4
Page 7 of :o Page B ol 10
- --- --.. -.. -.. -- ---...
MAR.WK1 MAR.WK1
GAO.JNOWATERMONH-LYMONrTOANG: GRO'J-.Cf'iATEH r REATMENT Pl.NIT
(1) NEATER SYSTEM
RAINFALL OAT A
MAA.1995
DATE CHEStOAY
ITEM INFLUENT EFFLL-"NT %RED.
03/01 /95 0.00
03/02/95 0.00 FLOW -TGD 2.3 2.3
03/03/95 0.25
03/04/95 0.00 COD mgll 6808.1 159.0 97.7%
03/05/95 0.40
03/06/95 0.00 TSS mgll 15.1 30 .. 0
03/07/95 0.00 ..
03/08/95 0.60 LOW 5.2 7.1
03/09/95 0 .. 00 pH
03/10/95 0.00 HIGH 5.7 B.3
03/11/85 0,00
03/12/95 0.00
03/13/95 0 .. 00 GAOI...U)WATEA TREATMENT Pl.ANT
03/14195 0.00 (2) OUTER TEA SYSTEM
03/15/95 0.00
03/16/95 0.00
03/17/95 0.00
03/1 8/95 0 .. 00
03/19/95 0.00
ITEM >FLLENT EFFLL-"NT %RED. (
03/20/95 0.50 FLOW • TGD 85.4 85.4
03/21 /95 0 .. 00
03/22/95 0.00 TSS mgll 3.9
03/23/95 0 .. 00
03/24/95 0.00 LOW 5.5 6.0
03/25/95 0.00 pH
03/26/95 0.00 HIGH 5.B 7.0
03/27/95 0.00
03/28/95 0.00
03/29/95 0.00
03/30/95 0.00
03/31/95 0.00
0.44
0.60
0.00
Page 9 of 10 Page 10 of 10
---- -----.. ---.. ---
MARREF.WK1
DALY REFER ENO:: 9-!EET:
DATE: IT. EQ PLT. CEO DEC. W,S "°' M• "" NIT FHlS "°' FIM -NF. TNK SEP. lK) LO LQ ADV ;..oo lK) w,s 5/DAY
1995 coo COO. coo = Tf.S TSS ,..,. NIT FHlS GALS LBS S<T. GALS FIM AVG.
5050 6050 4910 226 14< 12640 2476 115 11.8 3 95 57 0.18
5650 5700 5800 235 112 11900 2296 1t 1 16.6 3 100 67 0.22
5500 5950 4490 237 120 13460 2416 125 22.8 100 57 0.17
4 5195 6180 6410 248 112 13600 2440 130 24.0 " 54 0.23
5 6710 5960 6090 231 116 12400 2448 134 25.0 1 100 65 0.22 0.20 • 6170 6220 6090 207 104 12840 2600 93 13, 7 3 120 62 0.21 0.21
6740 6310 5860 166 56 15760 2520 134 10,6 3 110 54 0.21 0.21
8050 4640 4540 140 72 150BO 2628 112 25.3 1 11 0 ,. 0.15 0.20
4920 4970 5770 130 40 14440 2416 120 16.2 2 100 65 0.21 0.20
10 6250 5520 541 0 120 BO 15300 3004 118 13.8 3 130 81 0.18 0,19
11 6850 6000 6100 135 104 14140 2516 119 14.4 2 3 135 75 0.22 0.19
12 7200 6300 8250 145 84 13860 2364 132 20.0 1 115 81 0.24 0.20
13 7130 7100 6730 135 24 17180 2728 138 10.3 2 3 110 73 0.22 0.21
14 6260 6320 5890 110 32 17220 1872 1'0 30.1 1 1 110 105 0.28 0.22
15 6210 5760 5710 108 48 18840 2920 130 17.0 2 2 115 81 0.17 0.22
18 5560 -1950 6160 150 58 15660 2600 138 12.2 2 115 78 0.20 0.22
17 8010 8100 8360 175 ,o 17760 2784 128 17.0 3 120 83 0.20 0.21
1B 6780 8250 7900 135 .. 17400 2800 130 20.0 3 120 100 0.25 0.22
19 8050 8730 5810 175 98 17200 2840 125 111.0 2 125 135 0.18 0.20
20 8520 8380 61-10 190 BO 15480 284-1 15' 12.8 2 2 130 " 0.19 0.20
21 7150 7445 6180 180 " 17780 33-10 162 22.7 125 100 0.16 0.20
22 6150 6000 5800 170 " 170-10 2888 159 21.0 125 " 0.18 0.19 (
23 6700 6070 6170 165 .. 15200 3088 149 7 .3 3 3 115 1 05 0.18 0.18
24 7700 6000 5800 185 .. 15220 3020 166 15.3 1 130 108 0.17 0.18
25 6800 6400 6200 150 88 15680 2796 158 16.0 3 125 100 0.20 0.18
26 6550 6350 6500 180 120 14980 2724 154 19.3 1 3 125 108 0.21 0.19
27 12370 7560 6550 180 100 \6600 3146 1'4 ,., 3 3 130 97 0.19 0.19
2B 12171 9250 15600 3480 155 17 .8 1 125 62 0.15
29 6440 7560 8430 190 52 17120 3364 188 20.6 2 2 120 108 0.22 0.16
30 6590 6950 6780 305 108 17160 3160 168 23.9 1 120 100 0.19 0.16
31 8970 7430 3890 185 72 16600 5400 153 ,.o 0 130 100 0.06 0.13
AVG: 6851 6464 6023 17< 81 15527 2643 138 17.3 2 117 65 0.20 0.19
MAX: 12370 9250 8430 305 14' 18640 5400 188 30.1 3 135 135 0.26 0.22
MN: 4920 4640 3890 108 24 11900 1672 " 7 .3 0 95 54 0.06 0.13
Pag9 1 011
-
N'RL
1995:
-
il -1
04/01 /95 240
04/02/95 244
04103/95 244
04/04/95 242
04/05/95 241
04/06/95 238
04/07/95 236
04/08/95 236
04/09/95 235
04/10/95 234
04/11 /95 229
04/12/95 225
04/13/95 232
• 04/1 .. /95 232
04/15/95 223
04/16/95 233
04/17/95 229
04/18/95 1 85
04/19/95 223
04/20/95 219
04121195 220
04/22195 215
04/23/95 210
04/24/85 204
04/25/95 198
04/26/95 197
04/27/95 197
04/28/95 189
04/29/95 194
04/30/95 198
AVG: 221
TOT: 6642
-
IT-2
78
70
00
70
78
77
75
75
74
73
73
71
72
71
88
70
60
50
86
68
71
70
70
60
60
87
68
65
68
60
71
2137
-
IT-3
181
164
185
182
185
180
177
175
176
181
144
158
188
180
155
183
185
132
162
162
180
168
183
158
150
157
158
140
150
150
164
4934
- -
WELLS.WK1
IT-4
200
225
201
181
263
287
245
103
246
236
104
204
210
210
2'1
232
261
148
217
204
196
188
186
200
178
172
251
1 81
1 BJ
221
212
ffiERTER
DAILY FLOW:
IT-5
297
316
290
256
196
144
141
113
80
117
85
OJ
85
78
81
02
02
01
132
211
250
268
259
228
270
275
230
210
214
226
IT-6
223
226
230
224
221
170
173
216
206
122
0
1
0
0
0
0
0
122
167
101
107
207
217
211
205
204
202
190
100
106
6361 5436
150
2896
-
ff-7
211
200
220
100
200
102
101
187
185
183
181
100
211
207
182
202
100
164
160
127
121
122
122
120
120
110
74
87
57
51
159
4773
-
348
258
171
0
20
129
274
278
140
0
227
237
220
57
0
0
0
177
250
283
200
288
207
200
202
8
0
245
280
287
177
5314
-
IT-9
0
0
0
0 •• 454
508
318
0
0
1024
468 ••• 1128 ••• 1112
378
620
887
707
782
773
744
687
711
721
321
167
12
5
488
14650
1825
-- -----
WELLS.WK1
OUTEATEA
DAILY FLOW:
APRL
1995: OT-1 OT-2 OT-3 OT-4 OT-5
04/01/95 21400 23714 2092 1375 2507
04/02/95 22300 24621 2137 1414 2562
04/03/95 22600 25630 2144 1431 2531
04/04/95 20600 28150 1990 1444 2597
04/05/95 17200 29854 2030 1427 2633
04/06/95 15500 28106 1949 1433 2601
04107195 19100 27811 2124 1452 2323
04/08/95 21400 24940 2135 1459 2274
04/09195 22500 26980 2029 1460 2434
04/10195 22700 27640 2042 1459 2395
04/11/95 22000 27230 2143 1447 2127
04/12/95 21400 28244 2059 1446 1989
04/13/95 22000 28292 2107 1458 1945
04/U/95 22100 27561 2108" 1463 1931
04/15/95 21700 27511 2103 1472 2114
04/16/95 21000 26363 2115 1454 2118
04/17/95 20800 28551 1975 1457 2239
04/18/95 18000 30832 2078 1475 2284
04/19/95 16000 30441 2075 1468 2233
04/20/95 20000 28419 2059 1462 2180
04/21/95 22500 28244 2150 1476 2144
04/22/95 22600 28829 2083 1480 2212
04123/95 22500 28801 2156 1486 2237
04/24/95 22100 28526 2125 1484 2207
04/25195 22100 28859 2130 1488 2189
04/28195 22100 28884 2101 1478 2189
04127/95 22400 29481 2136 1475 2212
04/28/95 20900 27287 2050 1430 2116
04/29/85 18800 25700 2075 1538 2139
04/30/95 14400 30655 2110 1570 2414
AVG: 20697 27672 2087 1462 2269
OT-6
6653
6863
6977
71 25
7034
704 5
6762
6793
7012
7048
7004
7075
7088
7088
7028
6868
7152
7258
7176
7086
7216
7224
7181
7127
7139
71 21
7192
6798
6602
71 77
7031
-
OT-6A
6136
6364
6497
6837
6986
6977
641 2
6204
6492
6536
6438
6565
6549
6602
6443
6266
6683
6916
6819
6683
6816
6834
6844
6753
6760
6775
6752
6224
6124
6862
6605
--
OT-7 OT-8
2416 18200
2499 19000
2539 19200
2602 19500
2578 18500
2577 18000
2465 16700
2461 17600
2545 18300
2563 18400
2552 18100
2585 18400
2587 18500
2582 18600
2566 18400
2511 18000
2602 19000
2635 18400
11611 16000
2564 14 700
2630 13900
2630 13000
2647 11800
2597 11400
2613 11400
2613 10200
2642 11900
24 72 20900
2420 20400
2614 22200
2864 16953
TOT: 620900 836156 62610 43861 68076 210918 188161 85919 508600
87840
- --- --
ITMAINT1.WK1
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
"-"ER TEA SYSTEM
ACTION
DATE LOCATION PRJ!l.EM DATE
04/14/95 CAUSTCP\JMP COITN....ESTORUN 04/17/95
04/18/95 IT-6 low Flow 04/18/95
04/18195 IT-8 low Flow 04/18/95
04118/95 IT-9 Low Flow 04/18/95
Page 1 of 1
- --
ACTION MECHi\NIC
REPAIRED START STOP m
SWITCH
FE PLACED CONTROl.S JP PP PW
a.EAM:D Pl.MP SCREEN JP PP PW
FE SET CCNTRO..S JP PP PW
-- --------
-- - - --
OTMAINT1.WK1
MAINTENANCE ACTIVrTIES-GROl.R'IIOWATER OPERABLE UNIT #1
OUTER TIER SYSTEM
DATE LOCATK>N
04/1 B/95 IT·S
04'24/9 5 IT-1
PfUll.EM
LOW FLOW
LOW FLOW
ACTION
DJ.TE
04118/95
04/24/95
Pe.ge 1 or 1
--- -- -- - -----
ACTION MEO-Wa::;
SET FLOW JPPPPW
a...EMEO SCREEN JP PP PN
--- -- - -- -- - --- -----
RAINFALL.WK1
GROUf',OWATER MONTHLY MONrTOAh\G:
RAINFALL DATA
DATE INCHEOOAY
04/01/95 0.00
04/02/95 0.00
04/03/95 0.00
04/04/95 0.00
04/05/95 0.00
04/06/95 0.00
04/07/95 0.00
04/08/95 0.00
04/09/95 0.00
04/10/95 0.00
04/11/95 0,00
04/12/95 0.10
04/13195 0.00
04/14/95 0.00
04/15/95 0.00
04116/95 0.00
04/17/95 0.00
04/18/95 0.00
04/19/95 0.30
04/20/95 0.10
04/21/95 0,00
04/22/95 0,00
04/23/95 0.90
04/24/95 0.00
04/25/95 0.00
04/26195 0.00
04/27/95 0.00
04/28/95 0.00
04/29/95 0.00
04(30/95 0.00
TOTAL 1.40
AVG 0.35
Pege 1 of 1
---- -- - --- ---- -----
APRILWK1 APRIL.WK1
GAOONJWATER MONTHLY MONITORN3: GAOLNJWATEA MONTH. Y MONrfORING:
NER TIER COMBINED INFLUENT #2 ITCI OUTER TIER COMBINED t-FLLENT: #1OTCI
PAGE t-0.1 PAGE00.1
APRIL:1995 APRIL 1995
DATE: FLOW: PH COO: T&;: TOC: DATE: FLOW: PH: TDC:
GD pH ppm ppm ppm GD pH ppm
04101/95 1396 5.4 10840 8 04/0'1/95 84493 5.6
0 4/0 219 5 1422 5.3 11090 10 0 4/0 2/9 5 B7760 5.5
04/03/95 1621 5.3 10100 11 04/03/95 89549 6.0
04/04/95 1273 5.4 13320 115 04/04/95 91045 5.8
04/05/95 1146 5.3 12310 31 04/05/95 88253 6.0
04/06/95 597 5.1 13130 102 3566 04/06/95 84188 5.8 5.8
04/07/95 1473 5.2 13450 46 04/07/95 85149 5.7
04/08/95 1524 5.3 10700 67 04/08/95 85266 5.8
04/09195 1092 5.3 10000 28 04/09/95 89752 6.3
04/10/95 790 5.2 12790 208 04/10/95 90783 6.0
04/11/95 2157 5. 1 10340 93 04/11/95 89041 5.6
04/12/95 1589 5.5 5480 20 04/12/95 89763 5.9
04/13/95 1974 5.5 10630 68 3053 04/13/95 90526 6.0 6.1
04/14/95 2088 5.3 8150 12 04/14/95 90033 5.5
04/15/95 1741 5.4 6830 10 04/15/95 89337 5.3
04/16/95 2104 5.3 6300 15 04/16/95 86695 5.5
04/17/95 1106 5.3 5600 20 04/17/95 76343 5.6
04/16/95 1582 5.1 14460 59 04/18/95 89878 7.1
04/19/95 1955 5.2 6890 5 04/19/95 93823 5.5
04/20/95 2180 5.3 6230 20 1671 04/20/95 85153 6.1 2.9
04/21/95 1898 5.3 6310 3 04/21/95 87076 5.9
04/22/95 2009 5.2 6000 7 04/22/95 86892 5.9
04/23/95 1988 5.2 6700 11 04/23/95 85662 5.9
04/24/95 1868 5.1 6450 10 04/24/95 84319 5.8
04125/95 1926 5.1 6550 15 04/25/95 84678 5.6
04/26/95 1692 5.2 6750 9 0 4/26/9 5 83461 5.9
04127/95 1216 5.2 7400 1 4 3014 0 4/27 /9 5 86190 6.2 4.0
04/28/95 1237 5.3 12160 17 04/28/95 90177 5.8
04/29/95 1094 5.4 10360 10 04/29/95 85798 5.7
04/30/95 1117 5.3 10720 10 04/30/95 90002 5.6
AVG: 1562 5 9268 35 2826 AVG: 87370 6 5
MAX: 2180 6 14460 208 3566 MAX: 93823 7 6
MJN: 597 5 5480 3 1671 Mt-J: 76343 5 3
Page 1 of 10 Page 2 of 10
------- ---- --- -----
APRILWK1 APAILWK1
GAOJM)WATER MrnTH... Y MONITOR~: GFtC>I.IDWATER MONTH.. Y MONrTORING:
SBA MIXED LIOLkJR: Sll™L AFTI:RF\.ATE SEPAPATOA BEFORE SBA:
PAGE NO. 4 PAGE N0.3
APRIL 1995 SF.TT. SLu:v·_£ ,. , ..... ., '-J/UMf APRIL 1995
DATE: PH: NH3N: P04: DO: MLSS: MLVSS: sa..RJS: WASTED FIM: F/M: DATE: PH: COO: TSS:
pH ppm ppm ppm ppm ppm ml/I min relio ratio pH ppm ppm
04/01/95 8. 1 150 18.4 1.7 3496 125 195 0.20 04/01/95 6.4 7770 36
04/02(95 8.0 142 20.4 .5 3200 120 130 0.24 0 4/0 2/9 5 6.2 8570 44
04/03195 7.9 146 25.4 7 2984 130 121 0.19 04/03/95 5.3 6500 40
04/04/95 8.0 142 18.2 1 5 2984 125 120 0.18 0. 16 04/04/95 6.0 5920 16
04/05/95 7.9 138 31.8 1.6 2808 1640 125 143 0.15 0. 19 04/05/95 5.7 4660 44
04/06/95 8.0 129 14.8 .3 2916 125 97 0.17 0. 19 04/06195 5.6 5710 12
04/07/95 8.0 139 17.8 .3 3412 125 121 0.15 0 17 04/07/95 5.5 5850 12
04/08/95 8.0 178 23.6 .6 3068 115 108 0.17 0 16 04/08/95 5.7 5950 20
04/09/95 8.0 168 22.4 .9 3012 110 110 0.19 0.17 04/09/95 5.7 6550 28
04/10195 8.0 123 19.3 .9 2884 125 92 0.18 0.17 04/10/95 6.2 5880 20
04/11/95 8.0 148 23.8 4 3022 125 75 0.14 04/11/95
04/12/95 8.1 190 19.6 0.6 3012 1680 105 90 0.17 0.14 04/12/95 5.7 5690 24
04113/95 8.0 167 22.5 1.7 4520 120 108 0.14 0.14 04/13/95 5.6 7060 48
04/14/95 8.0 273 17.9 2. 1 3484 125 110 0.14 0.13 04/14/95 6.1 5320 36
04/15/95 8.1 240 18.0 1.9 3360 125 105 0.14 0.12 04/15/95 6.2 5240 40
04/16/95 8.0 165 19.6 .8 3120 125 150 0.16 0.15 04/16/95 6.9 5500 24
04/17/95 8.1 124 22.0 1.8 2908 120 110 0.17 0.15 04/17/95 6.8 5450 40
04/18/95 7.9 117 10.0 1.8 3220 125 67 0.12 04/18/95
04/19/95 8.0 126 32.3 2.5 2424 1652 110 90 0.18 0.13 04/19/95 6.6 4910 20
04/20/95 8.0 126 28.6 0.6 2972 125 108 0.15 0.13 04/20/95 6.7 5150 72
04/21/95 7.9 103 1 1. 2 1.8 2504 110 108 0.23 0.15 04/21/95 6.4 6400 32
04/22/95 8.0 150 35.4 1.9 2948 125 110 0.19 0.15 04/22/95 6.3 6300 20
04/23/95 8.0 147 32.0 2.1 2976 125 100 0.18 0.19 04/23/95 6.7 6100 32
04/24/95 8.1 108 15.7 2.3 3376 120 108 0.15 0.18 04/24/95 6.2 5700 40
04/25/95 7.6 141 25.8 1.9 2664 125 97 0.18 0.19 04/25/95 6.0 5450 44
04/26/95 7.9 171 23.4 2.4 2868 2420 125 100 0.17 0.18 04/26/95 6.2 5560 48
04/27/95 7.7 140 25.0 2.0 2696 130 108 0.19 0.18 04/27/95 6.6 5750 28
04/28/95 7.9 148 26.0 2.3 3444 125 121 0.15 0.17 04/28/95 6.4 5770 36
04/29/95 7.8 139 22.1 2.0 3360 125 40 0.14 04/29/95
04/30/95 7 .9 142 24.0 1.9 3200 130 108 0.22 0.15 04/30/95 6.1 8080 14
0.11
AVG: 8 151 22 2 3095 1848 122 108 0.18 0.15 AVG: 6 6037 32
MAX: 8 273 35 3 4520 2420 130 195 0.24 0.19 MAX: 7 8570 72
MIN: 8 103 1 0 1 2424 1640 105 40 0.14 0.11 MIN: 5 4660 12
Page 3 of 10 Page 4 of 10
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APRIL.WK1 APA1l.WK1
GROONDWATER MONTH....Y MONITOR!~: GROLNJWATER MONTl-1. Y MONrTOR1/\K3:
SBA EFFLUENT:(OECANT) #4 SBAE INNER TIER EQUALIZATION TANK: !TEOT
PAGE NO. 5 "PAGF.N0.2
APRIL 1995 WAS. NH3N PH()S. APRIL 1995
DATE: FLOW: COO: TSS: TSS ADDED: ADDED: DATE: PH: CCO: OT WATER ADDED
Cf!) ppm ppm ppm gal lbs pH ppm gal
04/01/95 2138 179 40 15020 2 2 04/01/95 7.0 7680 200
04/02/95 2169 221 76 15600 2 2 04/02/95 7.1 8460 650
04/03/95 2061 175 72 16080 04/03/95 7.1 7430 866
04/04/95 2255 198 64 17320 3 04/04/95 7.1 7740 452
04/05/95 2158 210 40 12140 1 1 04/05/QS 7.0 7600 464
04/06/95 2225 180 48 16200 2 2 04/06/95 7.0 7790 825
04/07/95 2193 175 52 16420 2 .2 0 4/0 7 /9 5 6.9 7210 600
04/08195 2299 175 88 16300 0 4/0 8/9 5 6.8 6300 400
04/09/95 2262 170 84 16660 1 04/09/95 7.1 6600 709
04/10/95 2277 165 72 16820 2 04/10/95 7.3 7640
04/11/95 160 44 16280 1 04/11/95 7.5 8010
04/12/95 2145 165 64 16600 1 2 04/12/95 6.9 7350
04/13/95 2253 125 68 15840 2 2 04/13/95 7.0 7450
04/ 1 4/95 2140 140 64 20880 04/14/95 7.4 6560 440
04/15/95 1830 156 56 39200 0 04/15/9S 7.2 5390
04/16/95 2166 160 80 17800 0 04/16/95 7.1 5600 550
04/17/95 2216 156 132 15600 0 4/ 17 /9 5 6.6 5460
04/18/95 155 120 15000 04/18/95 5.6 6960
04/19/95 2241 145 20 16120 04/19/95 9.3 6530
04/20/95 2307 166 106 16400 04/20/95 6.6 6410
04/21195 2275 155 24 15580 2 3 04/21/95 6.3 6020
04/22/95 2284 165 52 12720 , 04/22/95 7.1 5850
04/23/95 2302 165 96 13400 1 04/23/95 7.2 5800 460
04/24/95 2190 187 48 14820 2 2 04/24/95 7.1 5380 540
04/25/95 2263 205 40 12440 , 04/25/95 6.0 5350 410
04/26/95 2245 224 44 12880 04/26/95 6.2 5610 621
04/27/95 2244 255 100 14340 04/27/95 6.2 5600 922
04/28/95 2359 279 96 16940 04/28/95 6.4 5630
04/29/95 04/29/95 6.3 7050
04/30/95 2094 321 -112 16400 3 3 04/30/95 '6.2 8160
AVG: 2207 185 68 16476 1 1 AVG: 7 6687 569
MAX: 2359 321 132 39200 3 3 MAX: 8 8460 922
MIN: 1830 125 20 12140 0 MN: 6 5350 200
DID t-OT PRCX:E:SS SBR
Page 5 of 10 Page 6 of 10
--- -- - -- --- --- ---- -
APRILWK1 APRIL.WK1
GROUNDWATER MOOTH.. Y MONITORING: GROl..tOWATER MONTH. Y MONITORIIIJG:
INt,IEATIERCARBON Fl.TEA EFFLUEITT OUTER TIER CARBON FL TEA EFFLUENT:
PAGE NO. 7 #8 lTEF P.A.GE !'.:O. 3
APRIL 1995 APRIL 1995 #7 OTEF
DATE: P!-!: = TOC: TSS: DATE: PH: TOC: TSS:
pH ppm ppm ppm pH ppm ppm
04/01/95 04/01/95
04/02/95 04/02/95
04/03/95 04/03/95
04/04/95 04/04/95
04/05/95 8.2 200 33 04/05/95 5.8 0.2
04/06/95 51.4 04/06/95 3.5
04/07/95 04/07/95
04/08/95 04/08/95
04/09/95 04/09/95
04/10/95 04/10/95
04/11/95 04/11/95
04/12/95 8.2 160 04/12/95 7.7
04/13/95 49.0 04/13/95 4.1
04/14/95 04/14/95
04/15/95 04/15/95
04/16/95 04/16/95
04/17/95 04/17/95
04/18/95 04/18/95
04/19/95 8.3 130 04/19/95 6.2
04/20/95 28.4 04/20/95 2.3
04/21/95 04/21/95
04/22/95 04/22/95
04/23/95 04/23/95
04/24/95 0 4/24/9!
04/25/95 04/25/9
04/26/95 8.4 207 04/26195 8.2
04/27/95 26.4 04/27195 3.2
04/28/95 04128/95
04/29195 04/29195
04130195 04130/95
AVG: 8 174 39 33 AVG: 6 3 0.2
MAX: 8 207 51 33 MAX: 8 4 0.2
MIN: 8 130 26 33 MN: 6 2 0.2
Page 7 of 10 Page 8 or 10
-- - -
GRa.Jf,OWATER MOflH. Y MOOITORN3:
RAINFALL DATA
DAlE 11"-CHESr'DAY
04/01/95 0.00
0 4/0 2/9 5 0.00
04/03/95 0,00
04/04/95 0.00
04/05/95 0.00
04/06/95 0,00
04/07/95 0.00
04108/95 0.00
04/09/95 0.00
04/10/95 0.00
04/11/95 0.00
04/12/95 0.10
04/13/95 0.00
04/14/95 0.00
04/15/95 0.00
04/16/95 0.00
04/17/95 0.00
04/18/95 0.00
04/19/95 0.30
04/20/95 0.10
04/21195 0.00
04/22/95 0.00
04/23/95 0.90
04/24/95 0.00
04/25/95 0.00
04/26/95 0.00
04/27/95 0.00
04/28/95 0.00
04/29/95 0.00
04/30/95 0.00
1.40
0.35
-- - ---
APAIL.WK1
Page 9 of 10
--
APA.1995
ITEM
FLOW -TGO
COD -mg/L
TSS mg/L
LOW
pH
HIGH
ITEM
FLOW -TGD
TSS
pH
mg/L
LOW
HIGH
- --_,_ - -
(1)
APRIL.WK1
GROUM)WATER TREATMENT PLANT
NERTF.R.SYSTEM
INFLUENT EFFLUENT %RED.
1.6 1.6
9268 174,3 98.1%
35.1 33.0
5.1 B.2
5.5 B.4
GAOUt-OWATER TREATMENT PLANT
(2) OUTERTERSYS1EM
NFLUENT EFFLUENT % RED.
87.4
5.3
7.1
87.3
0.2
5.B
7.7
Page 10 ol 10
OOTES
DO r-DT PRCCESS
04/11 /95 04/18/95
AND 04/29/95 LOW
WATER LEVEL IN E.O.
TANK. SEVERAL INNER
TIER WELLS LOW OR NO
FLOW.
-- ---- - --- - --- --·---APRIL.REF.WK1 OAA. Y AEFHHU SHEET: DATE: n. EQ PLT, DEC CK WAS MX "' MX "' e,a;MX F/~.I APffi ,,., TNK SEP. LIO ''" LC ,,._DU ADD LO WAS 510/\Y UQ5 coo cro CC!J. CCG. ,ss. TSS ""' "" FK6 <WS LBS SET. 0"-5 F<M .VO 10840 7680 7770 179 " 15020 3496 '" 18.4 2 2 m "' 0.20 11090 8460 8570 22, " 15600 3200 \42 20.4 2 2 120 130 0.24 I 01 00 7'130 6500 "' 72 16080 2988 "' 25.4 1 1 "' 121 0.19 • 13320 7740 5920 "' .. 17320 21184 \42 18.2 1 3 m 120 0.18 ' 123 \0 7600 "'660 210 " 121◄ 0 2808 136 31.8 1 1 m "' 0.15 o. to 1 3 I 30 7790 5710 160 " 16200 2916 129 1'1.8 2 2 m " 0.17 O. IO 13450 7210 5850 "' 52 16420 3412 "' 17 .8 2 2 m 121 0.15 0.17 10700 6300 5950 "' " 16300 3068 178 23.6 1 1 "' 100 0.17 0.16 • \0000 6600 6550 170 .. 16660 3012 "' 22.4 1 1 110 110 0.19 0.17 10 12790 5640 5880 165 72 \6820 288<1 123 19.3 2 1 m " 0.18 0.17 " 10340 8010 160 .. 16280 3020 "' 23.B 1 1 m 75 0.14 12 5480 7350 5890 "' " 16600 3012 190 19.6 1 2 "' 90 0.17 0. 14 " 10630 74 50 7060 m " 15840 4520 107 22.5 2 2 120 100 0.14 0.14 " 81 50 6560 5320 1'0 " 20880 3<184 273 17.9 1 1 m 110 0.14 0.13 " 8830 5390 5240 "' " 311200 3380 2'0 18.0 0 ' m 105 0.1"' 0.12 16 6300 5600 5500 160 " 17800 3120 "' 111.8 0 ' m 150 0.16 0.15 17 5600 5480 54 50 "' 132 15800 2908 "' 22.0 1 1 120 110 0.17 0.15 " 14460 81180 "' 120 15000 3220 117 10.0 1 1 m " 0.12 " 88110 8530 010 "' " 18120 2424 "' 32.3 1 1 110 90 0.18 0.13 20 8230 6410 5150 "' "' 18400 21172 "' 28.8 1 1 m 100 0.15 0.13 21 8310 6020 8400 "' " 15580 2504 10, 11.2 2 ' 110 100 0.23 0.1 5 22 6000 5850 8300 10, 52 12720 211"'9 150 35.4 1 1 m 110 0.111 0.1 S 23 6700 5800 8100 "' .. 13400 21178 1'7 32.0 1 1 m 100 0.18 0.111 " 64 so 5380 5700 107 .. 14820 3378 106 15.7 2 2 120 100 0. 1 S 0.18 25 6550 5350 54 50 '" " 12UO 2664 1'1 25.8 1 ' m 97 0.18 0.111 26 6750 5810 5560 "' .. 12880 2868 171 23.4 ' ' m 100 0.17 0.18 27 HOO 5800 5750 "' 100 14340 26116 1'0 25.0 ' ' 130 100 0.111 0.18 26 12160 5630 5770 279 .. 161140 3H4 "' 26.0 1 1 m 121 0. 15 0.17 29 10360 7050 \6200 3360 "' 22.1 1 1 "' " 30 10720 8160 8080 '" 112 16400 3200 m 24.0 3 ' 130 106 0.22 0.15 31 AVG: 11268 6621 6037 "' .. 18467 30115 151 22.2 1 1 122 106 0.18 1#,)( 1"'460 8460 8570 321 132 311200 4520 273 35.4 3 ' 130 "' 0.24 MN 5480 5350 4660 m " 12140 2424 "' 10.0 0 1 105 " 0.1"' P11g11 1 of 1
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Attachment 4
Data Quality Assessment Summary
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DATA VALIDATION REPORT
FOR
ANALYSIS OF GROUNDWATER
AT
HOECHST CELANESE
SHELBY, NORTH CAROLINA
Prepared for
Kubal-Furr & Associates
7821 N. Dale Mabry Hwy.
Suite 106/206
. Tampa, Florida 33614
May 1995
KF A Purchase Order
Verbal from Jerry Kubal
Prepared by
A2EC
Ankerberg & Associates Environmental Consultants, Inc.
1864-A 56th Place South
St. Petersburg, Florida 33712
813-866-9312
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TABLE OF CO.NTENTS
SECTION PAGE
1.0 INTRODUCTION
2.0 FIELD DATA
l
2
3.0
4.0
5.0
ANALYTICAL DATA VALIDATION 4
3 .1 TCL /TCLP Volatile Organics -Method 8240 4
3.2 Drinking Water Volatile Organics -Method 502.2 9
3.3 TCL /TCLP Semivolatile Organics -Method 8270 11
3.4 Drinking Water Semivolatile Organics -Method 525 15
3.5 TAL /TCLPMetals and Chromium -Method 6000 and
7000 series
3.6 TCL /TCLP Pesticides -Method 8080
3.7 Drinking Water Pesticides/PCBs -Method 505
3.8 Ethylene Glycol by GC/FID
3.9 TCLP Herbicides by EPA Method 8150
3.10 Total Organic Carbon Analysis
TABLES
17
20
25
28
29
30
4.1 Results of Analysis for TCL and TCLP Volatile Organic Compounds
Using Method 8240 (3 Pages)
4.2 Results of Analysis for DW Volatile Organic Compounds in
Groundwater Using Method 502.2
4.3 Results of Analysis for TCL and TCLP Semivolatile Organic
Compounds Using Method 8270
4.4 Results of Analysis for DW Semivolatile Organic Compounds in
Groundwater Using Method 525
4.5 Results of Analysis for T AL and TCLP Metals in Groundwater and
Sludge
4.6 Results of Analysis for TCL and TCLP Pesticides/PCBs Using Method
8080
4.7 Results of Analysis for DW Pesticides/PCBs in Groundwater Using
Method 505
APPENDICES
Appendix A -Semiannual Ground-Water Sampling Matrix (February)
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1.0 INTRODUCTION
Thirty one (31) ground-water samples, two waste water treatment system influent and
effluent sarnples, and two sludge samples were collected from monitoring wells, residential wells
and two wastewater treatment systems located at the Hoechst Celanese, Shelby, North Carolina
facility between March 6, l 995 and March 9, l 995. These samples were collected as part of the
facilities semiannual ground-water monitoring program. The samples were collected and analyzed
by !EA Laboratory in Cary, NC.
Twenty of the ground-water (twelve monitoring wells and four residential wells) and
treatment system (influent and effluent) samples and one SBR sludge sample were analyzed for
target compound list (TCL) volatile organic compounds (VOCs) by EPA Method 8240. Two (2)
treatm,~nt system effluent samples (IT and OT) and one SBR sludge sample were analyzed for TCL
semivolatile organic compounds (SVOCs) by EPA Method 8270, TCL pesticides and PCBs by EPA
Method 8080, and target analyte list (TAL) metals by EPA 6000 -7000 Series methods. The
ground.:water from the five (4) residential well samples were analyzed for total organic compounds
(TOC) by EPA Method 415.1, total chromium by EPA Method 6010, drinking water (DW) VOCs
?Y EPA Method 502.2, DW pesticides and PCBs by EPA Method 505, and DW SVOCs by EPA
Method 525. One (1) monitoring well ground-water sample (V23) and the IT treatment system
influent and effluent samples were analyzed for ethylene glycol by GC/FID. All of the monitoring
well and residential well ground-water samples and the treatment system samples were analyzed for
TOC. Both of the sludge samples were analyzed for full TCLP parameters (VOCs, SVOCs, Metals,
Pesticides/PCBs, and Herbicides). A schedule of the samples and the respective analyses are
presented in Appendix A, Section 5.0.
Results of the analyses were presented for data validation based on reduced deliverable
specifications. The U.S. Environmental Protection Agency (EPA) Laboratory Data VaEdation
Functional Guidelines for Organics (VOCs, SVOCs, Pesticides/PCBs) and Inorganics (Metals), Test
Methods for the Analysis of Solid Waste (SW-846), and the QC requirements specified by the
analytical method were used to conduct the data validation. Field data provided with the analytical
data have b,~en reviewed and the results are presented in Section 2.0. The results of the analytical
data validation are presented in Section 3.0 by parameter (subsections to section 3.0). All analytical
results and data validation qualifier codes have been presented in tables in Section 4.0.
In conducting the analytical validation, each analytical parameter has been evaluated in terms
of holding times, initial calibration, continuing calibration, method blanks, surrogate spikes (if
applicable), matrix spikes, matrix spike duplicates, sample duplicates (if applicable), laboratory
control samples, field blanks and trip blanks (if applicable). In the text, each analytical QC
parameter Gust described) is discussed. If found acceptable, the term "Acceptable" is written
adjacent to the title on the right side of the page; if found to have a discrepancy, the term "Qualified"
is written adjacent to the title on the right side of the page and the text discusses the dis·crepancy and
its effect upon the data. Data that is qualified as a result of the discrepancy are identified both in
terms of the required qualifying code, analytes and samples affected for both postive and non-detect
results.
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2.0 FIELD DATA REVIEW
The semiannual ground-water sampling and analysis program at Hoechst Celanese, Shelby,
NC required the measurement of depth to water in 93 different ground-water monitoring wells. At
the same time, ground-water samples were collected from 26 ground-water monitoring wells, 5
residential wells, and the influent and effluent from 2 water treatment systems. Two sludge samples
also were collected. All samples were collected and analyzed for selected chemical constituents by
!EA Laboratory. A schedule (Semiannual Ground-Water Sampling Matrix table) that lists the
identifications of wells to be sampled and those requiring only water level measurements is
prese•nted in Section 5.0 (Appendix A). During the field sampling, appropriate field records were
maintained and field tests were performed. A review of the field records was performed. The results
are presented below.
2.1
2.2
Water Level Measurement Log Acceptable
No record of a water level measurement was given by the laboratory for Monitoring well D-
56 (listed on the schedule presented in Appendix A). Conversely, a measurement for
monitoring well D-58 is presented on the laboratory water level measurement record. It is
suspected the identifications have been confused either by the laboratory or by the preparer
of the Sampling Matrix Table in Appendix A.
.Field Sample Logs Acceptable
A field sampling logs were collected for all samples, except sample D-56. This sample is
explained above. A water sampling log is presented in the field records for monitoring well
D-58. The indicated analytical parameters are TOC, pH, temperature, and specific
conductivity. No water sampling logs were prepared for the samples collected from the
water treatment systems (OTINF, OTEFF, ITINF, ITEFF). In addition, no sampling logs
w,~re provided for the sludge samples (SBR and FP). A request for sampling logs for these
samples should be submitted to the laboratory.
All sampling logs were examined for the following field sampling parameters and found to
be acceptable: Client name, client location, sample identification, field conditions, purge
date, purge time, purge volume, purge method, sampling date, sample matrix, sampling
method, field analyses (pH, temperature, specific conductance), test parameters, appropriate
sample container, container volume, sample preservative, container size, container number,
field team signature, and document completed in ink.
The sampling logs also were examined for the following information and it was not found
in the record: Sampling time, equipment decontamination procedures, and sample type (grab
vs. composite.
2
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I Section 2.0 Field Data Review
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2.3
2.4
Chain Of Custody Record Acceptable
All samples analyzed by the contract laboratory were submitted to the laboratory using
standard chain of custody record (COC) forms. The forms indicated the sample
identification, the date and time of collection, the sample matrix, and the requested analyses.
The number of sample containers is not noted on the COC. A total of five COCs were used
to submit the samples. The COCs all indicated the samples were received by the laboratory
intact, at a temperature of 4°C ± 2°. All COCs were signed by the laboratory sample
custodian.
Field Measurements Acceptable
All samples were tested for pH, specific conductance and temperature. No defects were
noted in these field measurements.
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3.0 ANALYTICAL DATA VALIDATION
The results reported for the analyses of collected samples have been validated according to
the National EPA Laboratory Data Validation Functional Guidelines for Organics and Inorganics
Analyses, the Quality Assurance Requirements specified by Chapter One of Test Methods for the
Analysis of Solid Waste, SW-846, Third Edition (Final), and the specific analytical QNQC
requirements specified by the method, where other guidelines are not available or applicable. The
results of analyses have been submitted under two sample delivery group numbers (SDG), 03195
and 03208. The validation for each analytical parameter is discussed separately below.
3.1 TCL !fCLP VOLATILE ORGANICS ANALYSIS BY EPA METHOD 8240
3.1.1 Data Presentation
All data has been presented for VOCs by 8240 with qualifier codes in Table 4.1 in Section
4.0. Samples analyzed by 8240 are listed in Appendix A. Also included are the SBR sludge
(totals analysis), and FP (TCLP Extract Analysis). A note from the lab (see insert, next page)
indicated the SBR TCLP VOC sample was not analyzed due to lab error.
3.1.2 Holding Times Acceptable
3.1.3 GC/MS Tuning Acceptable
Four GC/MS instruments were used for analysis and tuning with bromofluorobenzene (BFB)
prior to the analysis of any standards, samples or blanks was performed. All tunings were
within acceptance criteria.
3.1.4 Initial Calibration Acceptable
Four initial.calibrations were performed, one for each of four GC/MS instruments identified
lVISD5, MSD9, MSDI0 and MSDI I. Each are discussed below.
3.1.2. l Instrument MSDS
Two initial calibrations are reported, one for each SDG, 3 I 95 and 3208 performed on
3/16/95. Each has the same analysis date and time. This is acceptable, because the same
initial calibration was used for each SDG. However, a review of the individual calibrations
for each compound reveals that the relative response factors (RRFs) and percent relative
star1dard deviations (%RSDs) are different. No qualification of the data have been done
however, because both sets of data are within acceptable control limits. However, the
laboratory has been asked to explain this discrepancy.
Explanation: Laboratory explained that more than one set of calibration data were in the
GC/M:S computer at the same time to meet different client requirements. In processing the
initial calibration data for the different SDGs, two different calibration sets were used which
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3.1 TCL / TCLP voe ANALYSIS BY EPA METHOD 8240 CONTINUED
3.1.2.1 Instrument MSDS Continued
resulted in the different RRF and RSD results, i.e., the person processing the data,
erroneously selected the incorrect initial calibration data set for one of the calibraton sets.
3.1.2.2 Instrument MSD9 Acceptable
No comment. All RRFs and RSDs were within required control limits.
3.1.2.3 Instrument MSDl0 Acceptable
One initial calibration was performed for both SDG 3208 and 3195, on 3/15/95. The RRFs
for SPCC compounds were> 0.3 as specified by the method. Other analytes (acetone, 2-
butanone and 2-chloroethyl vinyl ether) had RRFs less than the 0.3. A reduced RRF on any
compound indicates a decrease in instrument sensitivity in detecting that compound.
However, because the method only specifies the criteria as applicable to SPCC compounds
no analytes are qualified. The %RSDs were acceptable for all compounds. Affected
samples are : TB36, FF62, C49, FF34, OTEFF, ITEFF, ITINF, OTINF, SBR, TB37,
VBLKJT, VBLKJU, SBRMS, and SBRMSD.
,3.1.2.4. Instrument MSDl 1 Acceptable
One initial calibration was performed for both SDG numbers, on 3/16/95. RRFs for SPCC
compounds were> 0.3 as specified by the method; RRF for 2-chloroethyl vinyl ether (0.255) ·
was < 0.3; However, _ because the method only specifies the requirement for SPCC
compounds no analytes are qualified. The %RSDs were acceptable for all compounds.
Affected samples are: VBLKK6, Lambert, Martin, VBLKKB, AA54, V23, V23MS,
V23MSD. See Table 4.1.
3.1.3. Continuing Calibration Acceptable
As with initial calibrations, each of the four GC/MS instruments analyzed samples under
separate continuing calibrations. Calibrations are discussed below for each instrument.
3.1.J.1. Instrument MSDS
Samples were analyzed under two continuing calibrations on 3/20/95 and 3/21/95
respectively.
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3.1 TCL / TCLP voe ANALYSIS BY EPA METHOD 8240 CONTINUED
3.1.3.1.1 Calibration 3/20/95 Acceptable
RRFs for SPCC compounds were> 0.3. RRFs for acetone (0.160), 2-hexanone
(0.180) and 4-methyl-2-pentanone (0.286) were < 0.3 criteria indicating a low
response of the instrument for these compounds. Percent differences (%Ds) for CCC
compounds were < 25% as specified by the method; %Ds for acetone (32.4), 2-
butanone (35.0), 4-methyl-2-pentanone (28. l) and 2-hexanone (30.9) were> 25%
criteria specified by the method. A reduced RRF on any compound indicates a
decrease in instrument sensitivity in detecting that compound. However, because the
method only specifies the criteria as applicable to SPCC compounds no analytes are
qualified. Also because %Ds for the CCC compounds are within the required limits
specified by the method, no data are required to be qualified. Affected Samples
are: EE58, T35, HH48, GG61, VBLKSZ
3.1.3.1.2 Calibration 3/21/95 Acceptable
RRFs for SPCC compounds and %Os for the CCC compounds are within the
required limits specified by the method. RRFs for acetone (0.238) and 2-hexanone
(0.271) were < 0.3 criteria specified by the method. A reduced RRF on any
compound indicates a decrease in instrument sensitivity in detecting that compound.
However, because the method only specifies the criteria as applicable to SPCC
compounds no analytes are qualified. Affected samples are: VBLK51, CC33,
PSS, K28, TB36.
3.1.3.2 Instrument MSD9 Acceptable
Samples were analyzed under two continuing calibrations, 3/16/95 and 3/17/95.
3.1.3.2.1 Calibration 3/16/95 Acceptable
RRF for SPCC compounds and %Ds for CCC compounds were acceptable. The
RRF for 2-hexanone (0.237) was< 0.3 criteria; %Ds were acceptable. A reduced
RRF on any compound indicates a decrease in instnunent sensitivity in detecting that
compound. However, because the method only specifies the criteria as applicable to
SPCC compounds no analytes are qualified. Affected samples are: VBLK93 and
TB35.
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3.1 TCL / TCLP voe ANALYSIS BY EPA METHOD 8240 CONTINUED
3.1.3.2.2 Calibration 3117/95 Acceptable
RRF for SPCC compounds and %Ds for CCC compounds were acceptable. The
RRF for 2-hexanone (0.244) was< 0.3 criteria; %Ds were acceptable. A reduced
RRF on any compound indicates a decrease in instrument sensitivity in detecting that
compound. However, because the method only specifies the criteria as applicable to
SPCC compounds no analytes are qualified. Affected samples are: VBLK95, Stein
and Walker.
3.1.3.3 Instrument MSDl0 Acceptable
Samples were analyzed under three continuing calibrations, 3/17/95, 3/19/95 and 3/27 /95.
3.1.3.3.1 Calibration 3117/95 Acceptable
Initial data submittal indicated too much time (greater than 12 hours) occurred
between the instrument tune with BFB and analysis of the continuing calibration
standard. Tune was shown to occur at 0850 hours with calibration occurring at 2122
hours. Discussion with laboratory indicated tune time actually occurred at 2050.
Supporting documentation was provided.
The RRFs for SPCC compounds and %Ds for CCC compounds were acceptable.
RRFs for acetone (0.247), 2-hexanone (0.283) were< 0.3 criteria; A reduced RRF
on any compound indicates a decrease in instrument sensitivity in detecting that
compound. However, because the method only specifies the criteria as applicable to
SPCC compounds no analytes are qualified.
¾Ds for chloroethane (66.8%)and 4-methyl-2-pentanone (25.6%) were > 25%
criteria. %D criteria is established by the method for Calibration Check Compounds
(CCCs) only. An elevated %D for any compound indicates the linearity of the
calibration curve for that compound may have shifted and, therefore, the quantitation
may be suspect. However, because the method only specifies the criteria as
applicable to CCC compounds no analytes are qualified. Affected samples are:
VBLKJT, TB36, FF62, C49, FF34, OTEFF, ITEFF, INTIN, OTINF.
3.1.3.3.2 Calibration 3/19195 Acceptable
RRFs for SPCC compounds and %Ds for CCC compounds are acceptable. RRFs
for acetone (0.225) and 2-hexanone (0.260) were <OJ criteria; %Ds were acceptable.
A reduced RRF on any compound indicates a decrease in instrument sensitivity in
detecting that compound. However, because the method only specifies the criteria
as applicable to SPCC compounds no analytes are qualified. Affected samples
are: VBLKJU, SBR, SBRMS, SBRMSD, TB37.
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3.1
3.1.4
3.1.5
3.1.6
3.1.7
3.1.8
3.1.9
TCL / TCLP voe ANALYSIS BY EPA METHOD 8240 CONTINUED
3.1.3.3.3 Calibration 3/27/95 Acceptable
RRFs for SPCC compounds and %Os for CCC compounds are acceptable. RRFs
for acetone (0.235), 2-chloroethylvinyl ether (0.235) and 2-hexanone (0.262) are<
0.3 criteria. A reduced RRF on any compound indicates a decrease in instrument
sensitivity in detecting that compound. However, because the method only specifies
the criteria as applicable to SPCC compounds no analytes are qualified. Affected
· samples are: VBLKJ2, FP
3.1.3.4 Instrument MSDl 1 Acceptable
Samples were analyzed under two continuing calibrations, 3/17/95 and 3/21/95
3.1.3.4.1 Calibration 3/17/95 Acceptable
RRFs for SPCC compounds were acceptable; RRF for 2-chloroethylvinyl ether
(0.255) was< 0.3 criteria; ¾Ds were acceptable. A reduced RRF on any compound
indicates a decrease in instrument sensitivity in detecting that compound. However,
because the method only specifies the criteria as applicable to SPCC compounds no
analytes are qualified. Affected samples are: VBLKK6, Lambert, Martin
3.1.3.4.2 Calibration 3/21/95 Acceptable
Surrogate Spikes Acceptable ·
Method Blanks Acceptable
Trip Blanks Acceptable
Matrix Spikes Acceptable
.,,.
Matrix Spike Duplicates and RPDs Acceptable
Summary
Except for the qualifications described above, all unqualified data is quantitative and may
be used for all purposes.
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3.2 DRINKING WATER voes ANALYSIS BY EPA METHOD 502.2
Ground-water samples from five residential wells were analyzed for drinking water volatile
organics by EPA Method 502.2. The results of the validation are presented below.
I 3.2.1 Data Presentation
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The data is presented with qualifier codes in Table 4.2 of Section 4.0. Samples analyzed by
method 502.2 are Lambert. Walker, Stein, Martin, and Elliott ( See Appendix A).
3.2.2 Holding Times Acceptable
3.2.3 Calibration Acceptable
The laboratory has stated that a single point calibration was performed. This is allowed
according to the method, Section 9.2.3, for continuing calibrations provided an initial 5 point
calibration has been successfully performed at some previous time. In discussion, the
laboratory stated they could not meet the ± 20% D criteria on continuing calibration, nor
could they obtain a successful five point curve with ¾RSD < 10%. Therefore, in
accordance with the method, a single point calibration was performed.
The laboratory agreed to provide evidence a successful five point calibration was performed
at a previous time that achieved the I 0% RSD for each analyte curve and that on
recalibration for the subject samples, achievement of the ± 20%D criteria was not possible
and performance of a new five point curve within the required time limits, that evidenced
an RSD less than 10% also was not possible. Based on this new information, no data are
required to be qualified. Affected Samples are: Elliott, Stein, Lambert, Martin, Walker
and Trip Blank.
3.2.4 Method Blanks Acceptable
3.2.5 Matrix Spike Acceptable
3.2.6 Matrix Spike Duplicate and RPD Acceptable
3.2.7 Laboratory Fortified Blank Acceptable
A laboratory fortified blank was analyzed according to the method and results are within
control limits.
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3.2 DRINKING WATER voes ANALYSIS BY EPA METHOD 502.2
3.2.8 Surrogate Spikes Qualified
One compound. fluorobenzene, was used as a surrogate spike. An aliquot of a solution of
this compound was spiked into all standards, blanks and samples. Two samples, Elliott and
Martin are reported with surrogate percent recoveries (¾R) that are high, outside the upper
control limits.
The obtaining of a surrogate spike ¾R that is outside control limits is an indication of
potential quantitation problems or matrix effects. Because the laboratory only used a single
point calibration technique, it is possible this may have affected the quantitation of
analytical results including the surrogate spike. However, because the laboratory fortified
blank results were within control limits, the cause of the high recovery is probably due to a
matrix interference.
An estimation of the amount of bias in affected samples in terms ofa percent error may be
obtained by subtracting the surrogate spike result from the upper control limit result and
dividing the difference by the upper control limit amount and multiplying the result by
100%. For example: If the surrogate spike control limit range is 90 -110 and the surrogate
result is 120. The minimum percent error bias is 9.09%. The maximum percent error bias
is 33.3% (determined by using the lower control limit). If the sample result is 7.8 with a 9%
positive bias, an adjusted result would be 7.2 derived by the following: 7.8 = X + 0.09X;
l .09X = 7.8; X = 7.8/1.09; X = 7. 16. Using the maximum bias the result would become 5.9
derived by the following: 7.8 = X + .33X; l.33X = 7.8; X = 7.8/1.33; X = 5.9. Because the
surrogate ·spike has a control range, rather than an exact true value, only an estimate of the
bias can be calculated and that also will have a range. The best estimate, using the above
example, is the result is between 5.9 and 7.2.
Positive results for all target compounds should be flagged "JK" as estimated, biased
high; non-detects have no effect. Affected samples are: Elliott, Martin. Because Elliott
has no postive result, it is unaffected.
3.2.9 Trip Blanks Acceptable
3.2.10 Summary .
Except for the qualifications described above, all unqualified data is usable for all purposes
as quantitative data.
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3.3 TCL / TCLP SEMIVOLATILE ORGANICS ANALYSIS BY EPA METHOD 8270
Two treatment system effluent samples (OTEFF and ITEFF) and one sludge sample (SBR
sludge) were collected and submitted for analysis of semivolatile organic compounds by EPA
Method 8270. The results of validation of these analyses are presented below.
3.3.1 Data Presentation
The data has been tabulated for these samples and is presented with qualifiers in Table 4.3
in Section 4.0. Samples analyzed by EPA Method 8270 are OTEFF, ITEFF, and SBR
Sludge (See Appendix A).
3.3.2 Holding Times Acceptable
All samples were extracted within seven days from the date of sample collection and
analyzed within 40 days from the date of extraction.
3.3.3 GC/MS Instrument Tuning Acceptable
3.3.4
3.3.5
Three instruments were used to analyze all samples. Tuning with
decafluortriphenylphosphine (DFTPP) was performed prior to the analysis of any standards,
blanks or samples.
Initial Calibration Acceptable
Three initial calibrations were performed, one on each of three separate GC/MS systems
identified as MSD4 on 3/21/95, MSD6 on 3/10/95, and MSD8 on 3/13/95. All SPCC and
CCC compounds were within the required >0.05 RRF and < 30% RSD criteria established
by the method. All compounds also were within these limits.
Continuing Calibration Acceptable
Three instruments were used to analyze all samples. Because some discrepancies occurred,
the Continuing calibrations are discussed by instrument and calibration date.
3.3.5.1 MSD4 -3/22/95 Acceptable .
One continuing calibration was done on this instrument on 3/22/95 for the analysis of HC
samples. All RRFs were acceptable. Percent differences (%Os) for 4-methylphenol (35.6%)
and benzyl alcohol (34.5%) exceeded the <30 %D criteria specified by the method. Neither
of these compounds are CCC compounds and the RRFs were good, indicating the instrument
response for detecting these compounds was acceptable. Because these compounds are not
CCC compounds, no data are required to be qualified.
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3.3 TCL / TCLP SVOCS ANALYSIS BY EPA METHOD 8270
3.3.5 Continuing Calibration Continued
3.3.5.1 MSD4 -3/22/95 Continued
Affected samples are: SVB251, SBR, SBRMS, SBRMSD
3.3.5.2 MSD6 Acceptable
Samples were analyzed under three continuing calibrations on 3/22/95, 3/23/95 and 3/28/95.
All RRFs and ¾Ds were within the acceptance criteria.
3.3.5.3 MSD8 Acceptable
Samples were analyzed under two continuing calibrations on 3/16/95 and 3/17/95.
3.3.5.3.1 Calibration 3/16/95
3.3.5.3.2 Calibration 3117/95
Acceptable
Acceptable
All RRFs were acceptable (i.e., <0.05); the %D for bis(2-chloroisopropyl) ether
(35%) was >30%D criteria; all ¾Ds for CCC compounds were< 30% (acceptable).
All RRFs were good indicating the instrument was able to detect the compound.
Because this compound is not a CCC compound, no data are required to· be
qualified. The user of the data is advised the results for bis(2-chloroisopropyl) ether
in affected samples are potentially suspect. Affected samples are: OTEFF, ITEFF,
OTEFFMS, OTEFFMSD
3.3.6 Surrogate Spikes Qualified
According to the EPA Laboratory Data Validation Functional Guidelines, data are not
qualified with respect to surrogate recovery unless "two or more surrogates within the same
fraction (base, neutral or acid), are out of specification. Under the second continuing
calibration of instrument MSD6, samples FP and FPSPK had one surrogate less than I 0%
R in the base/neutral fraction and three surrogates (all) less than 10% in the acid fraction.
Surrogat,~ recoveries in the method blank were acceptable. Results of the spiked compounds
in the FPSPK also showed low recoveries indicating the presence of a matrix effect.
Typically, based on these surrogate results the data must be qualified as unusable. However,
the presence of a matrix interference, evidenced by the results of the FPS PK can support a
lesser qualification of the data. Positive results for all compounds in affected samples
are flagged "J" (estimated); non-detect results are flagged "UJL" (estimated
quantitation, result biased low). Affected samples are: FP and FPSPK.
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3.3 TCL / TCLP SVOCS ANALYSIS BY EPA METHOD 8270
3.3.7 Matrix Spikes and Matrix Spike Duplicates Qualified
Two samples were selected for matrix spiking.
Sample SBR was spiked with matrix spiking compounds and analyzed as SBR, SBRMS and
SBRMSD. Out of eleven compounds spiked, five compounds (phenol, 2-chlorophenol, n-
nitroso-di-n-propylamine, 4-chloro-3-methyl phenol, and 4-nitrophenol) had ¾Rs high
and outside control limits in the matrix spike. Except for n-nitroso-di-n-propylamine, all
compounds were high, outside control limits in the matrix spike duplicate. All relative
percent differences (RPDs) were within control limits.
Sample OTEFF also was spiked with matrix spiking compounds and analyzed as OTEFF,
OTEFFMS and OTEFFMSD. Out of eleven compounds spiked, one compound, 4-
nitrophenol, was high, outside the control limits in both the MS and MSD. RPD's were
acceptable.
The functional guidelines specify that no action is taken in MS/MSD data alone. However,
using informed professional judgement the data reviewer may use the MS/MSD results in
conjunction with other QC criteria and determine the need for some qualification of the data.
Based on the quality of the calibrations, surrogate spikes and method blanks, no
qualification of the data based on the MS/MSD results is recommended except in those
samples spiked (SBR and OTEFF)
Positive results for the matrix spike compounds out of control in both samples should
be flagged "JK" as estimated, biased high; non-detects for these compounds require no
actfon.
3.3.8 Method Blanks Acceptable ·
Five method blanks (one for full SVOCs, four for TCLP SYOCs) were extracted and
analyzed with the samples. These are identified as SYB251, SVB258, SYB256, TCLP 238,
and TCLP 239. All were free of any detectable analytes.
3.3.9 Summary
Except for the qualifications described above, all unqualified data is quantitative and may
be used for all purposes.
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3.4 DW SVOCS ANALYSIS BY EPA METHOD 525
Ground-water samples from five residential wells (Lambert, Walker, Stein, Martin and
Elliott) were analyzed for drinking water semivolatile organics by EPA Method 525. The results of
the validation are presented below.
3.4.1
3.4.2
Data Presentation
The data is tabulated with qualifier codes and presented as Table 4.4 in Section 4.0. Samples
analyzed by this method are Lambert, Walker, Stein, Martin, and Elliott. See Appendix A.
Holding Times Acceptable
All Samples were extracted within 7 days from the date of collection and analyzed within
40 days from the date of extraction.
3.4.3 GC/MS Tuning Acceptable .
3.4.4 Initial Calibration Qualified
A single five point calibration was performed that is applicable to all samples. The RRFs
for all compounds were acceptable; the ¾RSD for pentachlorophenol (45.2%) and simazine
(44.6%) were >30%, other compounds were acceptable.
Positive results for these compounds are flagged "J" ( estimated); non-detect results for
these compounds are unaffected and remain unqualified. No positive detects were
reported so no action is required.
Affel'.ted samples are: Lambert, Walker, Stein, Martin and Elliott
3.4.5 Continuing Calibration Qualified
A single, one point mid-range calibration was performed applicable to all samples. The RRF
for pentachlorophenol was 0.01~ which is< 0.05 criteria used for Method 8270 or CLP
Method 625-CLP-M; the ¾Os for pentachlorophenol (82.5) and dibenz(a,h)anthracene (32.8)
were > 30% D and are unacceptable. Method 525 has no specified criteria for RRF
performance; method 525 does require ¾Os to be< 30%. The data must be qualified.
Positive results for these compounds are flagged "J" (estimated); non-detect results for
pentachlorophenol are qualified and flagged "UJL" as estimated quantitation, biased
low; non-detect results for dibenz(a,h)anthracene are unaffected and remain
unqualified because of good RRF performance.
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3.4
3.4.6
3.4.7
DW SVOCS ANALYSIS BY EPA METHOD 525
Method Blank Acceptable
Surrogate Spikes Qualified
One surrogate spike (p-terphenyl-D14) was used to spike all samples. Method 525 specifies
only one surrogate is required and others may be used. However, the recommended
surrogate compound specified by the method is perylene-D12. The use of other surrogates
such as caffeine-15N2 and pyrene-D10 also are suggested. The use ofp-terphenyl-D14 is
recommended as an optional recovery standard to check on the recovery of the internal
standards and surrogates in the extraction process. The addition of terphenyl-D 14 to the
extract is optional, and is recommended for use in monitoring the recovery of the internal
standards and surrogates in fortified blanks and samples. The method does not indicate p-
terphenyl-D 14 to be used as a surrogate spike for monitoring analyte recovery in samples.
One sample, Martin, had surrogate recovery, low, outside control limits. Other
samples surrogate recoveries were acceptable.
The evaluation of the surrogate recovery when only one surrogate compound is used,
especially in the analysis of semi volatile organic compounds, which involve both basic and
acidic fractions, presents a difficult professional judgement assessment. No validation
criteria are available ( other than the method) as guidance. Generally, more than one
surrogate is used for the analysis of base, neutral and acid extractables analysis. Typically,
three surrogate compounds for each fraction are used. The rules governing surrogate
recovery also are fairly strict and specify that data are not qualified with respect to surrogate
recovery unless two or more surrogates, within the same fraction are out ·of specificati.on,
unless recovery is less than l 0%. Thus, the use of only one surrogate makes evaluation
difficult. This difficulty is further compounded when the surrogate used is not a surrogate
compound specified by the method. In addition, because the matrix spike and matrix spike
duplicate data are identified as a "batch" specific MS/MSD, no information about the
presence of a matrix interference can be inferred and applied to the surrogate recovery.
Therefore, evaluation can only be based on the available data. The Martin sample must be
qualified as follows:
Positive results for all compounds in affected samples are flagged "JL'' as estimated,
low bias; non-detects are flagged "UJL" as estimated quantitation limits, possible false
negative.
Affected samples are: Martin
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3.4 OW SVOCS ANALYSIS BY EPA METHOD 525
3.4.8 Matrix Spike/Spike Duplicate and RPDs Acceptable
A batch specific matrix spike and spike duplicate were analyzed. %Rs and RPDs were within
control limits. Because the MS/MSD is a batch specific spike, no assessment of matrix
effects is possible. The MS/MSD data may only be used to assess the analytical system
performance in terms of accuracy and precision.
3.4.9 Field Blanks Not Collected
No field blanks were collected or analyzed.
3.4.10 Laboratory Fortified Blank Acceptable
A laboratory fortified blank was analyzed in accordance with the method; all recoveries
were within control limits indicating method accuracy was acceptable.
3.4.11 Summary
Except for the qualifications described above. all unqualified data are quantitative and may
be used for all purposes.
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3.5 T ALffCLP METALS Ai'\/D CHROMIUM Ai'IAL YSES -METHOD 6000-7000 SERIES
Samples collected for target analyte list (TAL) metals analysis included the treatment system
samples (OTEFF, ITEFF and SBR Sludge). Samples collected specifically for analysis of chromium
are four of the residential well samples (Lambert, Walker. Stein, and Martin). These analyses were
a toial metals analysis. Two sludge samples, SBR Sludge and FP Sludge also were submitted for
analysis ofTCLP metals. Because TCLP metals extracts are analyzed by the same methods as total
metals analysis, the TCLP extracts were analyzed along with the other samples. Method blanks and
spike samples specific for TCLP analyses were included. However, the quality control data for the
TCLP metals is identical. Only the number of metals involved are reduced for the TCLP samples.
The metals analyses were divided into two analytical or sample delivery groups: SDG 3195, and
SDG 3208. The validation of these analytical data from these iwo SDGs is presented in two separate
reviews.
SDG 3195
3.5.1.A Data Presentation
All data has been tabulated with qualifier codes in Table 4.5. This validation is applicable
to samples FP (TCLP), FPMS (TCLP-matrix spike), FPMSD (TCLP-matrix spike duplicate),
TB#238(TCLP), TB#247(TCLP), ITEFF, Lambert, Martin, Stein, Walk, OTEFF, OTEFFD
(duplicate), OTEFFSD (spike duplicate).
3.5.2.A Holding Times and Sample Preservation Qualified
3.5.3.A
3.5.4.A
3.5.5.A
All samples for total metals analysis were preserved by reducing the pH of the
samples to less than 2 by using nitric acid. The pH of sample ITEFF was tested at
the laboratory and determined to have a pH of7,just prior to sample preparation. All
other samples for total metals analysis were adequately preserved with acid and had
pH values< 2.
Positive results for sample ITEFF are flagged "JL'' as estimated, biased low;
non-detect results are flagged "UJL" as estimated quantitation, possible false
negative.
Initial Calibration Acceptable
Continuing Calibration Acceptable
Method (Preparation) Blanks Qualified
An evaluation of calibration blanks and preparation blanks has revealed the presence
of some contaminants. Analytes of consequence for the samples include aluminum,
copper, and nickel. Other analytes were detected but either their qualifying amounts
were too low to be of consequence to any samples or the analyte was not detected in
the sample. Using the blanks 5x rule, the qualifying amounts for the above three
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3.5 T ALffCLP METALS Al"ID CHROMIUM ANALYSES -METHOD 6000-7000 SERIES
3.5.5.A Method Blanks Continued
3.5.6.A
3.5.7.A
3.5.8.A
3.5.9.A
3.5.10.A
SDG 3208
analytes are AL ([45), Cu (5.5) and Ni (14.0) respectively. Two samples are affected
by these analytes: OTEFF and ITEFF. OTEFF is affected by aluminum only.
ITEFF is affected by all three. The value for aluminum in OTEFF is 32.5. The
results for these three analytes in ITEFF are AL (129), Cu (2.4), and Ni (7;6).
In accordance with the functional guidelines, these results in both samples are
flagged "U" as non-detect.
Laboratory Control Sample Acceptable
Spike Sample Acceptable
Spike Duplicate RPDs Acceptable
Sample Duplicate RPDs Acceptable
Summary
Except for the qualifications described above, all unqualified data is quantitative and
usable for all purposes.
3.5.1.B Data Presentation
3.5.2.B
3.5.3.B
3.5.4.B
All data has been tabulated with qualifier codes in Table 4.5. This validation is
applicable to samples SBR (Totals), SBRD (Totals), SBRS (Totals),
SBRSD(Totals), SBR (TCLP), SBRMS (TCLP), SBRMSD (TCLP), TB#239
(TCLP).
Holding Times Acceptable
· Initial Calibration Acceptable
Continuing Calibration Acceptable
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3.5
3.5.5.B
3.5.6.B
3.5.7.B
3.5.8.B
3.5.9.B
TALffCLP METALS AND CHROMIUM ANALYSES-iYIETHOD 6000-7000 SERIES
Method Blanks Acceptable
No contaminants of concentrations sufficient to affect any samples either in the totals
analysis or in the TCLP samples were present in either the totals blanks or TCLP method
blanks.
Laboratory Control Samples Acceptable
Spike Sample Acceptable
Spike Duplicate RPDs Acceptable
Sample Duplicate RPDs Acceptable
3.5.10.B Summary
Except for the qualifications described above, all unqualified data is quantitative and usable
for all purposes.
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3.6 TCLrrCLP PESTICIDES & PCBS ANALYSIS BY EPA METHOD 8080
Two water treatment system samples (OTEFF and ITEFF) and one sludge (SBR) were
collected for total pesticides analysis by EPA Method 8080. One additional sludge FP also was
collected and submitted along with the SBR sludge for TCLP Pesticides analysis. The TCLP
Method also employs Method 8080 for analysis of the TCLP extract. Because the TCLP pesticides
list is much reduced (only 7 compounds) from the Method 8080 list of pesticides and because TCLP
pesticides extracts are analyzed by the same method (Method 8080) as total pesticides analysis, both
the total pesticides and TCLP pesticides extracts were analyzed together. Hence the quality control
data for the TCLP pesticides analysis is the same as the QC data for the total pesticides. Method
blanks and spike samples specific for the TCLP were included. The number of pesticides reported
for TCLP are reduced from the Method 8080 list in the TCLP samples. The pesticides analyses
were divided into two analytical or sample delivery groups: SDG 3195, and SDG 3208. However,
because of the lack of continuity in the QC documentation and the overlap of QC data between
SDGs, both groups are evaluated as one.
3.6.1 Data Presentation
3.6.2
All of the TCL Pesticides data has been presented with qualifier codes in Table 4.6 in
Section 4.0. The samples presented are: Total Pesticides, OTEFF, ITEFF, SBR; TCLP
Pesticides SBR and FP.
Holding Times Acceptable
All extractions were completed within 7 days of sample collection or TCLP extraction and
analysis of extracts was performed within 40 days of preparatory extraction. TCLP
extractions were completed within the required 14 days from date of sample collection.
3.6.3 Initial Calibration Acceptable
Two initial five point calibrations were performed and used for each SDG on two separate
instruments identified as HP5890P4 and HP5890P6. One initial calibration was performed
on instrument HP5890P4 on 3/18/95, the other initial calibration was performed on
HP5890P6 on 3/21/95. Retention times and calibration factors were determined and
presented on the FORM VI Pest-I and Pest-2 forms for each calibration. In the absence of
raw chromatograms or quantitation reports, an evaluation of the accuracy of these summaries
is not possible and may only be assumed.
It was noted that calibrations were not performed for the following compounds: chlordane,
toxaphene, and all Aroclors (PCBs). This was discussed with the laboratory. The
laboratory response was that because these were multicomponent (multi-peak) analytes, a
calibration of these compounds was not performed. Instead, a single standard of each of
these analytes was analyzed and compared to each of the samples. If any of these analytes
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3.6
3.6.3
TCLffCLP PESTICIDES & PCBS BY EPA METHOD 8080 CONTINUED
Initial Calibration Continued
appeared on the chromatograms of the samples. the laboratory would then go back and
calibrate for the detected compounds and reanalyze the samples. Because none of the
analytes were reported as detected in any samples, these calibrations were not performed.
The technique employed is not in accordance with the analytical method. However, the
laboratory provided chromatograms of the single concentration standard analyzed for
chlordane, toxaphene and the Aroclors and the sample chromatograms. A review and
comparison of the sample chromatograms with the standard chromatograms shows no
presence of the compounds. The review also shows the standards were analyzed on the same
instrument, during the same time frame as the samples, i.e., under the same instrument
calibration. The data are accepted. No qualification of the results for these compounds
is required.
3.6.4 Continuing Calibration Acceptable
All retention times were within the retention time windows for the compounds calibrated for
both instruments and for all continuing calibrations. The %Os for all compounds calibrated,
except for Endosulfan II in the continuing calibration performed on instrument HP5890P6
on 3/22/95, were less than or equal to 15% D criteria. The %D for Endosulfan [[ was 16.0
% and is greater than the required 15% criteria.
The non-detects for Endosulfan II are flagged "UJ" as estimated quantitation limit.
Affected samples are: OTEFF and ITEFF
3.6.5 Method Blanks Acceptable
Three total pesticide extraction blanks (PB555, PB550, and PB549) and two TCLP blanks
(TCLP238 and TCLP239) were analyzed with the samples. All were free of contamination.
3.6.6 Instrument Calibration Blanks Acceptable
All instrument Calibration blanks were free of contaminants.
3.6.7 Surrogate Spikes Acceptable
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3.6 TCLrfCLP PESTICIDES & PCBS BY EPA METHOD 8080 CONTINUED
3.6.8 Laboratory Control Samples Qualified
A laboratory control sample is a QC check sample comprised of a known concentration of
known analytes. This QC sample is analyzed along with other samples in the same manner
(extraction and analysis) and the results obtained are compared to the compounds and
amounts known to be present in the sample. If identifications and recoveries are not
consistent with the known sample, the analysis is considered to be flawed and an
investigation into the cause is undertaken. This investigation may include re-extraction, re-
calibration, and reanalysis of all associated samples.
Two laboratory control samples or Pesticide QC Check Samples were analyzed. These
samples were identified as LCS549 and LCS550. Both of these QC check samples were
analyzed on instrument HP5890P6. No QC check sample was analyzed on instrument
HP5890P4. Although not a requirement, good quality control practice would dictate these
QC check samples would be analyzed on different instruments.
Sample LCS549 had 2 compounds (delta-BHC [10%], and heptachlor [ll5%]) out of
18 compounds out of control. Delta-BHC was low, outside the control limits and
heptachlor was high, outside the control limits. Sample LCSSS0 also had two
compounds (delta-BHC [5%], and endosulfan I [145%1) out of 18 compounds out of
control. Delta-BHC was low, outside the control limits and endosulfan I was high,
outside the control limits. The qualification of the data in affected samples is presented
below.
For Delta-BHC, positive results would be flagged "JL'' as estimated, biased low. No
positive results are reported. The non-detects are rejected and flagged "UJL" as
estimated quantitation.
For hepatchlor and endosulfan I, positive results would be flagged "JK" as estimated,
biased high. No positive results are reported. The non-detects are unaffected.
Affected samples are: SBR, SBRMS, SBRMSD
3.6.9 TCLP Matrix Spikes Acceptable
3.6.10 TCL Matrix Spike, Matrix Spike Duplicate and RPDs Acceptable
Two matrix spike and matrix spike duplicates were performed using samples OTEFF and
SBR. Both samples were analyzed on instrument HP5890P6 like the LCS. Again, although
not a requirement, good quality control practice dictates it would have been bener for these
samples to have been analyzed on different instruments.
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3.6
3.6.10
TCLffCLP PESTICIDES & PCBS BY EPA METHOD 8080 CONTINUED
Matrix Spikes, Matrix Spike Duplicates and RPDs Continued
Sample OTEFFMS had five compounds (beta-BHC [200%], delta-BHC[l4%], heptachlor
[145 %], aldrin [130%], and 4,4'-OOE [285%]) out of 18 outside control limits. All but
delta-BHC were high, outside control limits. Sample OTEFFMSO had 11 compounds (beta-
BHC[ 270%], heptachlor [190%], aldrin [175%], heptachlor epoxide [145%], endosulfan I
[180%], dieldrin [165%], 4,4'-OOE[405%], endrin [150%], 4,4'-000 [160%], endosulfan
sulfate [200% ], and methoxychlor [ 170%]) out of 18 outside control limits.
Affected samples are: ITEFF and OTEFF
Sample SBRMS had six compounds (beta-BHC [415%], delta-BHC [0%], gamma-BHC
[135%], dieldrin [700%], 4,4'-OOE [0%], and endrin aldehyde [0%]) out of 18 outside
control limits. Sample SBRMSO had nine compounds (alpha-BHC [36%], beta-BHC
[550%], delta-BHC [0%], gamma-BHC [135%], aldrin [125%], endosulfan I [170%],
dieldrin [9500%], 4,4'-OOE [550%], and endrin aldehyde [0%]) out of 18 outside control
limits.
Affected samples are: SBR
Matrix spike data are generated to determine long-term precision and accuracy of the
analytical method on various matricies. These data alone cannot be used to evaluate the
precision and accuracy of individal samples and/or to invalidate/validate data. Control limits
are advisory. No action is taken on MS/MSO data alone to qualify an entire case. However,
using informed professional judgement, the data reviewer may use the MS/MSO results in
conjunction with other QC data and determine the need for some qualification of the data.
In making evaluations, the reviewer must first try to determine to what extent the results of
the MS/MSO affect the associated data. As shown, a large percentage of the analytes spiked
have percent recoveries outside the control limits. Some of these recoveries are consistently
low, and some are consistently high. Failures for some of the same analytes also occurred
in the LCS. However, the surrogate spikes had acceptable recoveries in each sample for all
surrogate compounds and method blanks were free of contaminants ..
The failures presented in the MS/MSO data may be due: (1) to matrix interferences; (2) a
problem within the extraction and analytical system that affects analyte detection and/or
quantitation: or (3) poor spiking technique by the laboratory. Based on the available data,
(recoveries are both low and high, and surrogate recoveries are in control) it does not appear
that a matrix interference is present. Because recoveries are both low and high it appears
more likely that the cause for the MS/MSO failures is poor spiking technique by the
laboratory. No action is taken.
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3.6 TCLffCLP PESTICIDES & PCBS BY EPA METHOD 8080 CONTINUED
3.6.11 Summary
Except for the qualifications described above, all unqualified data are quantitative and may
be used for all purposes.
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3.7 DRINKING WATER PESTICIDES & PCBS BY EPA METHOD 505
Ground-water samples from five residential wells (Lambert. Walker, Stein, Martin and
Elliott) were analyzed for drinking water pesticides & PCBs organics by EPA Method 505. The
results of the validation are presented below. .
3.7.1 Data Presentation
All of the DW Pesticides & PCB data have been presented with qualifier codes in Table 4.7
in Section 4.0. The samples presented are: Lambert, Walker, Stein, Martin, and Elliott).
3.7.2 Holding Times Acceptable
3.7.3
All extractions were completed within 7 days of sample collection and analysis of extracts
was performed within 40 days of extraction.
Initial Calibration Qualified
A six point calibration was performed. Relative response factors are> 0.05 and the percent
relative standard deviation is< 10% for all calibrated compounds except dieldrin (14.4%),
heptachlor epoxide (11.0%), and hexachlorocyclopentadiene (10.2%).
Also, it is noted that calibration data for alachlor, atrazine, chlordane, simazine,
toxaphene and all aroclors are not provided although these compounds are reported as non-
detects for the samples. This was discussed with the laboratory. The laboratory response
was that "compounds alachlor, atrazine, and simazine were not calibrated because they are
not part of!EA's usual NC Drinking Water 505 compound list. They were not analyzed for
with the set of standards that were run. The data for these three compounds actually was
reported from the Method 525 analysis. These data are therefore rejected in terms of being
part of method 505 but are noted as valid for method 525. Qualification and flagging is
presented below.
As to chlordane, toxaphene and aroclors, the laboratory stated that because these
compounds were multicomponent (multi-peak) analytes, a calibration for these compounds
was not performed. Identification of these compounds is based on pattern recognition and
the retention times of key peaks. Instead of calibrating for these compounds, the laboratory
stated that a single standard of each of these analytes was analyzed and compared to each of
the san1pks. If any of these analytes were to appear on the sample chromatograms, the
laboratory would calibrate for the detected compounds and reanalyze the samples. Because
none of the analytes were reported as detected in any samples, these calibrations were not
performed. Upon request, the laboratory provided a copy of the chromatograms for the
single concentration standards and for the samples. A review of the sample
chromatograms and the standard chromatograms confirms none of the pesticides in
question are present in the samples. The review also revealed the following:
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3.7 OW PESTICIDES & PCBS BY EPA METHOD 505 CONTINUED
3.7.3 Initial Calibration continued Qualified
(1) The samples were analyzed on March 24, 1995; The standards were analyzed on
several different days as follows: toxaphene (January 18, 1995), Aroclors (January 18,
26, 27, 1995, February 5, 1995), and chlordane (March 8, 1995); and,
(2) The samples were analyzed on a gas chromatograph equipped with a 30 meter DB-
608 column; the standards were analyzed on a gas chromatograph equipped with a 15
meter, DB-5 column. (These are equivalent to different instruments.)
It is the reviewers opinion, that the standard chromatograms provided by the laboratory for
this analysis are not related nor comparable to the analyses performed on the samples
because of the differences in columns, and times of analysis. Using the data provided, there
is no way to demonstrate that the 30-meter, DB-608 column used for the samples was
actually able to produce peak patterns similar to those typical for the pesticides and PCBs
in question. However, because the sample chromatograms do not show any evidence of
peak patterns typical of multi-peak pesticides or aroclors, the data will remain unqualified.
However, it is noted the methodology used by the laboratory is suspect and the laboratory
has been informed this technique unacceptable for future analyses. Based on the available
information, the data is qualified as follows:
On the qualification table (Table 4.7) all results for alachlor, atrazine and simazine are
flagged "UQl" and footnoted at the bottom of the table that the reported values were
obtained by method 525, not method 505.
Positive results for dieldrin, heptachlor epoxide, and hexachlorocyclopenfadiene, in
affected samples are flagged "J" as estimated; non-detect results for these analytes are
qualified and flagged "UJL" as estimated quantitation limit, possible false negative.
Non-detect results for toxaphene, chlordane and aroclors are flagged as "UQ2" and
footnoted at the bottom that the results are non-detect, based entirely on pattern
recognition, and analytical methodology is suspect.
Affected samples are: Elliott, Stein, Lambert, Martin, Walker and Blank
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3.7 OW PESTICIDES & PCBS BY EPA METHOD 505 CONTINUED
3. 7.4 Continuing Calibration Qualified
3.7.5
3.7.6
A single point mid-range standard is analyzed; RRFs are >0.05 and all ¾Ds, except for
heptachlor are < 15% as specified by the method. Also, as stated above for the initial
calibration, alachlor, atrazine, chlordane, toxaphene, simazine and the aroclors are not
calibrated. These data have already been qualified for the discrepancies in the initial
calibration. The same qualification applies to the continuing calibration. Additional
qualifications are presented below.
Positive results for heptachlor in all samples would be flagged "J" as estimated. No
positive results are reported. The non-detect results are unaffected because of a good
RRF.
Method Blank Acceptable
One method blank was provided. No contaminants were detected.
Surrogate Spikes Qualified
Two surrogate compounds were used as spikes, both are consistent with the method
requirements. One sample, Martin, had one surrogate recovery, decachlorobiphenyl, low,
outside control limits. This compound is an aroclor and the low surrogate recovery implies:
(I) a possible loss of analytical sensitivity for aroclors; (2) a matrix effect; (3) a problem with
sample extracti_on; or (4) poor spiking technique by the laboratory analyst. In the presence
of acceptable calibration data (for those compounds calibrated), good performance with
other surrogate spikes and good matrix spike performance, the _low surrogate recovery is
considered an isolated event and not indicative of a system wide problem. Because the
recovery is greater than 10%, no action is recommended.
3.7.7 Matrix Spike/Spike Duplicate and RPDs Acceptable
Nine compounds were spiked into a (presumed) reagent water blank (i.e., batch specific
MS/MSD). Percent recoveries in both the MS and MSD were within control limits and
RPDs, were acceptable. No estimation of matrix interference can be made from these data;
only evaluation of system accuracy and precision are possible.
3.7.8 Summary
Except for the qualifications described above, the unqualified data is quantitative and usable
for all purposes.
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3.8 ETHYLENE GLYCOL BY GC/FID
Three samples, one ground-water (V-23) and two treatment system samples (ITINF and
ITEFF) were collected for analysis of ethylene glycol by GC/FID. The results of the data validation
are presented below.
3.8.1 Data Presentation
A, no qualifier codes were required, the ethylene glycol data were not tabulated.
3.8.2 Holding Times Acceptable
3.8.3 Method Blanks Acceptable
3.8.4 Matrh Spikes Acceptable
3.8.5 Matrix Spike Duplicate and RPD Acceptable
3.8.6 Summary
Based on the available quality control information, the data is unqualified and classified as
quantitative. The data may be used for all purposes.
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3.9 TCLP HERBICIDES BY EPA METHOD 8150
Two sludge samples (SBR and FP) were collected and submitted for Full TCLP analysis,
including TCLP herbicides. The results of analysis for TCLP volatiles, TCLP semivolatiles, TCLP
pesticides, and TCLP metals have been presented in previous sections along with the totals analysis
for those parameters. No requests or samples were submitted for a total herbicides analysis,
therefore this section only presents the validation of the TCLP Herbicides.
3.9.1 Data Presentation
As no qualifier codes were required, the TCLP Herbicides data were not tabulated. All
results were non-detect.
3.9.2. Holding Times Acceptable
The FP sample was collected on 3/07/95. TCLP extraction for herbicides was performed on
3/14/95. Analytical preparatory extraction of the TCLP extract was performed on 3/20/95
and the sample was analyzed on 3/25/95. All holding times were within the 14day / 7day
I 40 day criteria from date of sample collection.
3.9.3 Initial Calibration Acceptable
3.9.4
3.9.5
3.9.6
3.9.7
3.9.8
A five point calibration was performed for all TCLP herbicide compounds. Retention times
and calibration factors for each compound at each standard concentration were determined
and are presented in the data.
Continuing Calibration Acceptable
All percent differences (¾Ds) of the calculated amount for each standard compound from
the nominal amount were less than the required maximum allowable 15% and all retention
times were within the control ranges for the retention time windows for each compound in
both the daily calibration verification summary and the continuing calibration verification
summary.
Instrument and Method Blanks Acceptable
Surrogate Spikes Acceptable
Matrix Spike Acceptable
Summary
Based on the available data, the data is classified as quantitative and may· be used for all
purposes.
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3.10 Total Organic Carbon
Thirty four groundwater samples were submitted for anaysis of total organic carbon (TOC).
These analyses were performed by the in-house Hoechst Celanese laboratory. All samples were
submitted with standard chain-of-custody forms. All samples were analyzed within 2 to 4 days of
sample collection meeting the required analytical holding time of 28 days. No field or quality
control data pertinent to these samples was provided. Addtional validation is not possible.
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4.0 DATA TABLES
4.1 Data Qualifier Codes
The following codes have been used to indicate various qualifications of the analytical data
for QC failures. All QC failures have been discussed in the text of the report. The definitions
provided below are generic.
CODE
u
J
JL
JK
R
UJL
UQl
UQ2
DEFINITION
Reported result is not detected at the indicated detection limit.
Reported result is estimated quantity; may be biased low or high due to one
or more QC failures.
Reported result is estimated quantity, biased low due to one or more QC
failures generally low outside control limits.
Reported result is estimated quantity, biased high due to one or more QC
failures generally high outside control limits
Reported result is rejected data and is considered unusable; rejection may be
due to severe QC failure or failure to follow analytical method. Rejected data
has been evaluated in terms of its potential admissability and defensibility in
a court of law.
Reported result was not detected at the quantitation limit and the quantitation
limit is estimated and biased low due to one or more QC failures.
Reported result is not detected at the quantitation limit; results were obtained
from analysis of sample by method 525, not method 505.
Reported result is not detected at the quantitation limit: results are based
entirely upon absence of typical pattern on chromatogram; methodology is
suspect and is unacceptable for any future use.
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-- -- - - ---- ----- -
Kulm I-Furr /\ssocic1tes
Hoecl1st Celanese
Semiannual GW Sampling
Table 4.1 Results of Analysis For TCL and TCLP Volatile Organic Compounds Using Method 8240
Parameters/Sample ID
Chloromelhane
Brornomethane
~~~XI chl?r_ide
Chloroethane
Methylene chloride
Acetone
Carbon dlsulfide
1, 1-DichiorOeihene
1, 1-0ichloroethane
1,2-0ichloroethene
Chlorororm
1,2-Dichloroethane
2-Butanone
Vinyl acetate
1.1, 1-Trichloroethane
Carbon tetrachloride
BiOrl1odichiOr-Onieitiane
1,2-0ichloropropane
VBLK5Z
10 U
10 U
10 U
10 U
SU
10 U
5ij
SU
SU
SU
SU
SU
10 U
SU
SU
SU
SU s u
cis-1,3-0ichloropropene 5 U
Trichloroethene 5 U
EE58
10 U
10 U
10 U
10 U
SU
10 U
SU
SU
SU
5U
SU
SU
10 U
su
SU
SU
5U
5U
SU
SU
T35 HH48 GG61
10 U 10 U 10 U
10 Li 10U iii Li
10 U. 10 U iii Li -·------·-----·-----·· -i6 u. -10 U 10 U
SU 5U SU
10 U 10 U 10 U ----. ----SU SU 5U .... --. ·--. SU SU 5U
SU SU SU
5U SU SU
5U SU SU
SU SU SU
.J:'Hf 12. 10 U 10 U
SU SU 5U
SU SU SU
iiu SU SU
SU SU SU
SU SU SU
SU SU SU
SU 170 SU
VBLK51
10 U
10 U
10 U
CC33
10 U
16" Li
iii Li
10 U 10 U
SU . 5LJ ..
1ou iau·
SU SU
SU SU
SU
SU
5U
SU
10 U
SU
SU
SU
SU
SU
5U
SU
SU
SU
5U . s Li
iii u
SU
SU
5U
P58 K28
10 U 10 U
iii u iii u·
10 u .. 16 u
10 u io u
SU SU
TB36
10 U
10 U
10 U
10 U
SU
VBLK93 TB35
10 U 10 U -·-10\j 10 u
10 U 10 U
10 U 10 U
5 Li s u
10 U 10 U 10 U 10 U 10 U
SU -·-·--···-···--·-·--· ··-· SU SU 5U SU
5U
5U
5U
SU
5U
10 U
SU
5U
SU
SU
SU
SU
SU
SU -------SU
ii Li su su
10 U
5U
SU .. iiu
SU
ii Li s Li
SU
·-·· SU
SU
5U
5U
SU
10 U
SU
SU
SU
5U
SU
SU
SU
su
SU
SU
SU
10 U
SU
5U su
SU
ii Li
SU
su·
SU
su
SU
ii u
10 U
SU
SU
SU
SU
SU
SU
-
Dibromochloromethane 5 U SU SU SU SU .. ---·-----· ··-··--· .. SU SU SU SU SU s u s u s u su ___ --su-_s_u_-+-_s_u_°"--s~u __ ,_ s u _____ EC:::. ---~LJ __ , __ _ --·· ..... ·--···---·--------... ·····-·---· 2-Chlt?_~oelhyl vinyl ether 5 U
1, 1,2-Trichloroethane 5 U ·
Benzene
lrans-1,3-0ichloropropene
Bromoform ·
4-ME!thYi-2-PentaOone
2-HexanOne - ·
SU
SU
SU
10 U
10 U
SU SU
5U SU SU 5U SU SU ··su ·· s u-· -·-·s u-·
SU SU SU SU · ii·u· ···--s··· s u 5 Li s u
SU SU SU -----. -. SU . . ··---------·-·--··-s u SU su· SU SU . ·---•----·-. ·-·· SU 5 U
SU SU SU SU
10 U 10 U 10 U
SU
10U 10U 10U
SU SU SU SU SU SU
10U 10U 10U. -10U 10U . 10U 10U __ , __ 10_U_, __ 10U 1ou·--·1ii·ir·---
-----~----I------·-··------10 U 1 o u __ °'1 o,,u=--1-....:..::10 u 1 o u -s·u-···--s u · -s u 5 u -5 u--··s u s u ·--·s-u--s u 5 u s u -s u -·--·-·· Telrachloroethene
s u s u s u --5 u s u s u s u s u s u s u s u · ---·5 u .. -. ·-.. 1, 1,2,2-T elrachloroelhane
Toluene --SU s·u··-· -·su SU SU SU 5U SU SU --SU -su·--·--5U
Chlorobenzene irn·--• . •--·SU SU SU 5 u·-·-···-·:rii------s·u-· -·!;-u---SU SU SU SU
~lhylbeni.en_e:···------·--SU SU SU SU . su···--·-·s·u SU SU SU 5U SU SU
St~rene --=-==}~:=. SLJ___ SU SU SU ~.LJ. __ · ~U ____ SU --5-U SU SU SU
Xylene SU S U S U S U sTi-·-SU SU S U SU SU · SU SU
'
Page 1
-
----Kubal-Furr Associates
Hoechst Celanese
Semiannual GW Sampling
Parameters/Samples I
Chloromethane
Bromornethane
Vinyl chloride
Chloroethane
Methylene chloride
Acetone
Carbon disulfide
1, 1-Dichloroelhene
1, 1-0ichloroethane
1,2-0ichloroethene
Chloroform
1,2-Dichloroethane ... . ... 2-Butanone
Vinyl acetate
1, 1, 1-Trichloroethane
Carbon tetrachloride
Bromodichloromethane
1,2-0ichloropropane
cis-1,3-Dichloropropene
Trichloroethene
Dibromochloromethane
2-Chloroethyl vinyl ether
1, 1,2-Tlichtoroethane
Benzene
~rans-1 !3-0ichloropropene
Bromoform
4-Methyl-2-Pentanone
2-Hexanone
T etrachloroethene ---. -1, 1,2,2-Tetrachtoroethane .. .
Toluene
Chlorobenzene
Ethylbenzene
Styrene
Xylene
~ \ Tlt.l ~ SAw-.(>L'-1
--- ------- -- -- -
Table 4.1 Results of Analysis For TCL and TCLP Volatile Organic Compounds Using Method 8240
VBLK95 Stein Walker VBLKJT TB36 FF62 C49 FF34 OTEFF ITEFF ITINF ~ OTINF
10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 20 U 10 U
iii t..i i Ii t..i -.... io t..i ··--···· -.
10 U 10 U 10 U 10 U 10 U 10 U 10 U 20 U 10 U
10 U 10 U 10 t..i. .. -. -10 U 10 U 10 U 10 U 10 U 10 U 10 U 20 U 10 U .. ...
10 U 10 U 10 U 10 U 10 U 10 U 10 U 1 () I ' •OU 10 U 10 U 20 U 10 U
5U 5U 5U 5U 5 t..i !iU 5U 5U SU 5U 10 U 5U
10 U 10 U 10 U 10 IJ iU U 10 U 10 U 10 U 10 U 10 U 220 10 U
5U SU 5U SU SU SU SU SU SU SU 17 SU
5U -s u· · SU .. . -··----.... -, . . . . ----··· -···· --· ---~ --------. SU SU SU SU SU SU SU 10 U SU --. --
SU SU SU SU SU SU SU SU SU SU 10 U SU
SU SU SU SU SU SU SU SU SU SU 10 U SU
SU 5U SU SU SU SU SU SU SU SU 10 U SU
SU SU SU SU SU SU SU SU SU SU 10 U SU ---. -------.. ----.. ---------· - --.. ---10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 36 10 U
SU SU SU SU SU SU SU SU SU SU 10 U SU
SU SU SU SU SU SU SU SU SU SU 10 U SU ---. ... --. SU SU SU SU SU 5U SU SU SU SU 10 U SU
SU SU SU SU SU SU SU SU SU Su. 10 U SU
su SU SU SU SU SU SU SU 5U SU 10 U s IJ
SU SU SU SU SU SU SU SU SU SU 10 U SU
SU SU SU SU SU SU SU SU SU SU 10 U SU
SU SU SU SU SU SU SU SU SU SU 10 U SU ---. -.. .
SU 5U SU SU SU SU SU SU SU SU 10 U SU
SU SU SU SU SU SU SU SU SU SU 10 U SU
SU SU SU SU SU SU SU SU SU SU 36 SU ----·· --------. ·---SU SU SU SU SU SU SU SU SU SU 10 U SU -··-... --. -------. -·--------· ·-·----· ... ----··· -·--. ·-----------. ····-----------. -.. ---. -.
SU SU SU SU SU SU SU SU SU SU 10 U SU
10 U 10 U 10 u ------...
10 U 10 U 10 U 10 U 10 U 10 U 10 U 20 U 10 U
10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 20 U 10 U -·. -· s~u ---. ·------.. --·------. ·-· ·--.
SU SU SU SU SU SU SU SU SU 10 U SU --· -------------· --• ------------------·------·-···-·-.. ··-------·-··. ---------. -·· -.. -.. ··---. -.
SU SU SU SU SU SU SU SU SU SU 10 U SU
···-·-··· . ----------· -· ----·--------------. ----------·----··-·· ------------.. ...
SU SU SU SU SU SU SU SU SU SU 10 U SU -·--SU SU SU SU SU SU SU SU SU SU 17 SU --·-SU SU SU SU SU SU SU SU SU SU 10 U SU -... ----.. --··-SU SU SU SU SU SU SU SU SU SU 10 U SU -.,. -. -----·· --------.. ·-... --· . ,. ------.. -........ -...
SU SU SU SU SU SU SU SU SU SU 10 U SU . -··---. -. -
.... -
.. -... -----. -·-·
.. -.. -------· --·--
\'::,1.?1"~•,,,> f'.hl: f"_ Cl = . ~~~ .. -·. .. ·-------.. -.. . ----..
Page 2
- - --Kubal-Furr Associates
Hoechst Celanese
Semiannual GW Sampling
Parameters/Samples
Chloromethane
BrOniomelhane
Vinyl chloride
Chloroethane
ME:~h.yl~~e c.hl~ri~~
Acetone
Carbon disulfide -. --~
1, 1-gichlor<?~lh~n~.
1, 1-J?!ch~or?_~l~~~e
~ ,?-Di~h-~?_r~eth~ne
Chloroform
1,2-Dichloroethane
2-Butanone
Vinyl acetate __ ~------··--·--_
1, 1, 1-Trichl~rc?~~~a_n_~--
Carbon tetrachloride
Bromodichloromethane
1 ~2-Dichloropropane _
~!~: 1 .. ~~~.!~~~-o_r?P~?P.~~~
Trichloroethene
Dibromoch1oromethane
2-Chloroethyl vinyl ether
--- ------- ---Table 4.1 Results of Analysis For TCL and TCLP Volatile Organic Compounds Using Method 8240
VBLKJU
10 U
10 U io u
10 u
5U
10 U
5U
5U
5U
5U
5U
5U
10 u
5U
SBR TB37 VBLKJ2 FP
10 U 10 U ---.. -----10 U 10 U
10 U 10 U 0.02 U 0.02 U
10 U 10 U
5U 5U ---. -... ------· 10 U 10 U --·stT -su
--···-·---~ ---------.. -----------5 U 5U 0.010U O.OlOU
5 U 5 U
5 U 5 U
5U
5U 5U
10 U 10 U
·0.610 u
0.010 U a 020 Li -. -------------··-----.. -----------5 U 5 U
0.010 U
0.010 U
0.020 U
5U 5U 5U
VBLKK6 ZHEB583 VBLKK6 Lambert Martin VBLKKB
0.02 U
0.010 U
0.010 U
0.010 U
0.020 U
10U 10U 10U 10U ----·--···---------·-------------------· 10U 10U 10U 10U
0.02 U
0.010 U
0.010 U
0.010 U
0.020 U
10 U
10 IJ -1,-0
10 U
5U
5U
5U
5U
·5 U
5U
10 U
10 U
10 U
5U ·--. -· ---- ------10 U
5U
5U
5U
5U
5U
5U
10 U
5 U 5 U ---t---c5c;Uc----J--5 U
...... -·-·--------
10 U
10 U
5U
11
5U
5U
5U
5U
5U
5U
10 U
5U
.
10 U
10 U
5U
10 U
5U
5U
5U
5U ---s u
5U
10 U
5U -·su
AA54
5U 5U 5U
5U
5U
0.010 U 0.010 U 0.010 U 0.010 U 5 U 5U
5U
5U
5U
5U
5U
5U
5U
5U
5U
10 U
10 U
10 U
ici u
5U
10 U
5U
5U
5U
5U
5U
5U
10 U
5U
5U
5U
5U
5U
5U
5U
5U
·-su
---·------·-5U
5U
5U
5U
5U
5U
5U
5U
5U
5U --------·---· 5U
5U
5U
5U
5U
5U
5U
ioTi 10 u
5U ------------·--·------------·-------·-5 U 0.010 U 0.010 U
5U
5U
5U
5U
5U
5U
10 U
0.010 U 0.010 U
0.010 U
0.010 U
5U
5U
5U 5U --------. 5U ·--5 U ---------------------------------···------------·----------0.010 U 5 U 5 U 5 U 5 U 5 U
5U
5U
5U
0.010 U 5 U
5U
5U
5U
5U
5 U 5 U
... -----5 U 5 U
.. -•----------··-----------·-·-··------_____ ,
5U
5U
5U
5U
5U
5U
5U
5U
5U
5U
5U 5U 5U
1, 1,2-Trichloroethane
Benzene
trans-1,3-Dichloropropene _
Bromoform
4-~ethyl-2-Pentanone _
2-Hexanone --·1ou--,--1~o~u-,---,ou·------,----··-·------10 u -1au··-·-1o·u---io·o-
5U
5U
5U
5U
5U
10 U 10 U 10 U 10 U 10 U
10 U
5U
5U
5U
Tetrachloroethene
~, 1,2,2-Tetrachloroe~h~~~
Toluene
5U
5U
5U
5U
5U
5U
5U 5U o.oiou o.oiou
5 U 5 U ···--------------5 U 5 U -------------------------------------------------5 U 5U 0.010U 0.010U -.. ------·. ------5U 5 U
5U 5U
Chlorobenzene
~thyl~~nzen~.
StY.r~ne _
Xylene .... -.. --------------··--·------·· --------·-------------·-· 5U 5U 5U
····-·---·· Footnotes:
1/ u code = anaiyte nOt deteCted at"rePOrteCfdeteCtion iiniit.
0.010 U
0.010 U
Page 3
. --·--------. --··----·-0.010 U 5U . --5 U
5U
0.010 U 5 U-
5U
5U
5U
5U
5U
5U ---------------·----5 U 5U
5U 5U
5 u
5U
5U
5U
5U
5U
5 U 5 U -·-------·-·---. 5 U 5 U
5U
5U
5U
5U
5U
5U
5U
5U
--
V23
10 IJ
10 U
10 U
10 U
5U
10 U
5U
5U
5U
5U
5U
5U
10 U
5U
5U
5U
5U
5U
5U
5U
5U
5U
5U
5U
5U
5U
10 U
10 U
5U
5U
5U
5U
5U
5U
5U
..
- ---
Parameter/Sample ID
Benzene
B,omobenzene
Brornochloromethane
Bromodichlorornethane
Brornoform
Bromomethane
n-Buty1benzene
sec-~uty!bc,1zene
lert-Butylbenzene
Carbon telrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane --· 2-Chlorotoluene
4-ChlorotOiuene
Dibromochloromethane
1,~-~!~~om0-3-chi?ropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
DichlorodiiluOromethane
1, 1-0ichloroethane
1,2-Dichloroethane
1, 1-bichloi-oeihene
cis--(2-DichiOrOeih€ne --
tr~n~-1,2-Di~hloro~thene
1,2-D!chlor~p~opane
1,3-Dichloropropane
~ ,2-~ic~ilor<:'P~ opane
1 ! 1-D(ch.l?r?pr?pene
cis-1,3-(?i~t~l<?ropropene
~a~s-1 _!?-~i~h~O~C!PfOP~!'1e
Ethylbenzene
Hexachlorobutadiene
ls_opr<;ipylb~n~ene
~-1s?propylt<;ill!e!'l~.
Methylene chloride
Naphthalene
Propylbenzene
~tyren_E:_: __ ~ -~--
1, 1, 1,2-Tetrach1oroethane
--- ---- - - -
Table 4.2 Results of Analysis for OW Volatile Organic Compounds In Groundwater Using Method 502.2
Kubal-Furr and Associates
Elliott
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U -· --· 0.50 U
0.50 U
0.50U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
o~o u
0.50 U
0.50 U
0.50 U
0.50 U
Hoechst Celanese Semiannual Groundwater Sampling
Stein Lambert Martin
0.50 U 0.50 U 1.3 JK
0.50 U
0.50 U
0.50 U
0.50 U
0.50U
0.50 U
0.50 U
0.50 U
0.50U
0.50U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 II
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U 0.50 U ------·· -----------0.50 U 0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 u
0.50.U
7.8 JK ...
0.50 U ---------
Walker Trip Blank Lab Blank
0.50 U 0.50 U 0.50 U
0.50 U
0.50 u
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50U
0 sou
0.50 u
0.50 U
0.50 U
0.50 U
0.50 u
0.50 U
050 u
0.50 u
0.50 U ··05ou
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50U
0.50U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50U
0.50 U
0.50U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U 0.50 U
0.50 U
0.50 Li
0.50 IJ
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50U a.sou
0.50 U a.sou
0.50 u
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 i.J
0.50 U
0.50 U
050 u
0.50 i.J
0.50 U
0.50 U oso u
050 u
0.50 U
0.50 U
0.50 u
0.50 U
0.50 U
0.50 U o sou
0.50 U osou
0.50 U
0.50 U
0.50 U 0.50 U
0.50 U
0.50 U
0.50 U
0.50 U ..
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
050 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 i.J ii:sou
0.50 U
0.50 u
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
0.50 U
-·----
0.50 U
0.50U
0.50 U
0.50 U 0.50 U
0.50 U 0.50 U
0.50 U 0.50 U
0.50 U 0.50 U
o.5o u o 50 ·u
0.50 U 0.50 U ·-·-··----------------0.50 U 0.50 U
Page 1
- ---
-- --- - -----------
Parameter/Sample ID
1, 1,2,2-Tetra<?h1<:>roethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene ______
1.~.~-Trichloro~~nzene
1, 1, 1-Trichl':)ro~lh~ne
1, 1,2-Trichloroethane
Trichtoroethene
T richloroftuoromethane ------·· ·---·--· -----·-· ...
~ .~.~-!~!~~-~~~~P.!~~an_~_
1,?,~-"frimet~yl~t::nz~ne
1,3,5-Trimethylbenzene
Vinyl chloride ro1ar Xyienes
Footnotes:
Table 4.2 Results of Analysis for OW Volatile Organic Compounds in Groundwater Using Method 502.2
Kubal-Furr and Associates
Hoechst Celanese Semiannual Groundwater Sampling
Elliott Stein Lambert Martin Walker Trip Blank Lab Blank -· ---·-··--------------0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U
0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U
0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U ----0.50 U 0.50 U o:so u .. 6.50 iT .. ··-····-·-· 0.50U 0.50 U 0.50U ----------------·-~----·--------------------·-· ·-·----------.,. ______ ,. -------------~---------------0.50 U 0.50 U 0.50 U 0.50U 0.50 U 0.50 U 0.50 U .
0.50 U 0.50 U 0.50 U 0.50 U . 0.50 i..i 0.50 U 0.50 U .. oso·u 0.50 U 0.60 U 0.50 U 0.50U 0.50 U 0.50 U
0.50 U 0.50U 0.50 U 0.50 U 0.50 u 0.50 U 0.50 U . ----------0.50 ii . ---. ··-··---
0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U ·• ------·------------····--------· ---------------·--·-·--------------
0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U .. ---------·· -------. 65ou ·-------·· ··-·-···-·----
0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U
0.50 U 0.50 U 0.50 U 0.50 U o:so u 0.50 U 0.50 ii
0.50 U 0.50 U 0.50 U 0.50 U 0.50 u 0.50 U ii.sou . ··------~--------------·----------------···•-0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U
·------------
..
-·····-··-·-·.
----
1/ U code = anatyte not detected at indicated detection limii;
2/ JK code = "reSull bi.ised h·igh due t()SUriOgaie SJ)ike ¾R~CovE!iy being hi9h, OUiSide contrOl iifliiis; ori1Y'"pOSi_tiVe resu1ts· attect~1; see Page 10 Of rePOrt;
·----------
----11----1----------···---------
------------1----1-
Page 2
----------.
.
- -
- -- -
Kubal-Furr and Associates
Hoechst Celanese
Semiannual GW Sampling
Parameter/Sample ID
Phenol
bis_( 2-Chloroethyl)ether
?-~~l~:m~e~~.n?! .
1,3-~ichloro_b~n-~E:ne
1,~-Di~h lo~<:>b_~~~~,~~
1,2-0ichlorobenzene -·····------····-----··-----
-- ----------T:3ble 4.3 Results of Analysis for TCL / TCLP Semivolatlle Organic Compounds Using Method 8270
SVB251
10 U
10 U
10 U
10 U
10 U
10 U ----------
10 U
SBR
110 JK
100 U
100 U
SVB25B
. -·----··---100 U
FP TCLP239 SBR
I
100 U
100 U
0.020 u 0.020 uji_ · 0.020 u 0.020 u
100 U ---------------------
SVB256 TCLP23B SVB251 OTEFF
10 U 10 U
10 U 10 U · ------·-·--·-·-· 1ou·---1ou
ITEFF
10 U
10 U
10 U ----------·---------· ----------· --------10 U 10U 10U
0.0,0U 0.020U iou· 10U 10U .. -..... ----·-· ---- -., .. 10U 10U 10U ·----------------------·--------·----·-·------· 10 U 10 U 10 U 2:Methylphe~ol _ _ _ ____ _ --•---·-- - . -----------------------· ----··---· ----·-------------------1----bis(2-~hlo,oi~opropyl)e!her
4-Methylphencl
N-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
lsophorone
2-Nitrophenol ___ _
2,4-Dirnelhylphenol
~i~(?_-_~!1_l?r~~tho!:Y)':1elh~~-e
?,~-O~~~lor~f:l~~~?I
1,2,4-Trichloro~enzene
Naphlh~l~n~
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-M~l~}'.lnapht~_?le~~
~~x~~h~~r~~Y~~~~~l?~.~E:~~ _
~!~.~-!~!~~~~!C?e~.E:~'?! ---
~.~ .. s-Trich~'?..'?P_~en':>1
?-Chloron~phthalene
2-Nitroaniline ---· ---...
i?i~E:t_t~ylph!I~_?.(~!~
':4-~e~aphth_yt1::n~ _
2,6-0inilrotoluene ---.. -
3-Nilroaniline
Acenaphthene _____________ _
~. ~-l?initrop~~n~I_
10 U 100U
10 U
10 U
10 U
10 U
10 U
10 U
100 U
100 U
100 U
100 U
100 U
100 U
0.020 U 0.020 UJL 0.020 U 0.020 U
0.020 U 0.020 UJL 0.020 U 0.020 U
-----·---· . ----------·--·----·--·-··---·------------10 U
10 U
10 U
10 U
10 U
20 U -----------
100 U
100 U
100 U
100 U
100 U
200 U
10 U --·---·-··-. ' -·------·--
0.020 U 0.020 U - -----•-.
0.020 U 0.020 U
10 U
10 u
10 U
10 U 10 ij-
10 U ----------------------
10 U ·--·--·--------------10 U ---·-·---···-··-·-------10 U
10 U 10 U -----·-----· 10 U 10 U
10 U 10 U
10 U 10 U
10 U 10 U
10 U 10 U
10 U 10 U --·-------·-10 U 10 U ·--·-·------. ------·------10 U 10 U ··--···-·--10 U 10 U
10 U 10 U
10 U 10 U . ---20 U 20 U --------·-10 U 100 U
200 U
0.020 U 0.020 UJL 0.020 U 0.020 U 0.020 U 0.020 U
10 U
10 U
20 U
10 U 10 U 10 U
20 U
10 U
10 U
100 U
100 U ·-•·------------------,__ ____ . ----------
10 U 100U -----·-··----· ---------·-· 10U 100U
10U 100U
50U 500U
10 U 100 U
0.020 U 0.020 UJL 0.020 U
0.020 U 0.020 UJL 0.020 U
0.020 U
0.020 U
20 U --,au· 10 U
10 u --· ---·1o·u ·
0.020U 0.020U 10U 10U
0.020 U 0.020 U 10 U 10 U
10 U 10 U ...... ------· 50U 50U
10 U 10 U
20 U
10 U
10 U
10 U . ----------
10 U
10 U
50 U
10 U --io u ··----ioo iT ----------------------------------------------------10 u 10 u -10 u
... ·---·-----------10 U 100 U ... --·-----· -50 U 500U
50 U
50 U
---------------· 1ou -iou-· ··10·0-·
. -·---------·-···· . -·····-------·---·-··· ---------·-------·-· -· ·-----·-·-----·-·--· ... ·--50 U 50U 50U
--10 U 10 U
50 U
50 U 50 U ~~~(tr~pt~E:~~1._
Dibenzofuran -------·-·-·----··----10 U 10 U
Page 1
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-
.
.
-
- ---- - -- -- -- -- --Kubal-Furr and Associates
Hoechst Celanese
Semiannual GW Sampling
Table 4.3 _Results of Analysis for TCL / TCLP Semivolatile Organic Compounds Using Method 8270
Parameter/Sample ID SVB251
4-Nilroaniline 50 U --·-.
4,6-0initro-2-methylphenol -1 _ ~~ U
N-Nitrosodiphenylaml~e -10 U
4-~rorn~phe~ylJ?!li:nyl~~~~~ .. ···-· !9 .. ~
Hexachlorobenzene -·---~!-:~!a~l~_l?_t~P!~~I~?~ _
Phenanthrene
Anthracene
[?i-n-butylphthalate
Fluoranthene
10 U
50 U
10 U
10 U
10 U
10 U
10 U
SBR
500 U
500 U
100 U
100 U
SVB258 FP TCLP239
--· --------
SBR SVB256 TCLP238 SVB251 OTEFF
50 U 50 U
10 U 1 /l I I ,o u
ITEFF
50 U
50 U
10 U
10U 10U 10U
100 U 0.020 U 0:020-UJL -6 026 u --6.620 U -,)026-iT --o.626T.i. --iou ___ --ioTi ·•· 10 u
500 U 0.020 U 0.020 LJjL 0.020 U
100 U -
100 U
100 U
100 u.
100 U
------• -. ·-· ------
0.100 U 0.100 U 0.100 U 50 U 50 U 50 U ---------------------·--·-----------·-----·-· ---------··· ·---10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10U 10U 10U ·····-------------·-···----------10 U 10U 10U
-
~yrene _
Bulylbenzylphlhalate _ _ _____ __!_Q_~ __ 1_1.'..:0:..::0c:U:._1 ____ _ <------'--' ----1-~~---------· ------· -----·--·------·-· 10 U 10 U 10 U ~. 3' -DichlorC??~~~id_i_n~
Benzo(a) anthr~~~~~ _
Chrysene
~is(2-Etllylhexyl)phlh~lat~
Di-n-octylphlhalate
Benzo(b)fiuoranlhene
~enzo(k)fiuorant~~en_~.
Benzo(a_)py~en~
I ~~eno( 1,? '. 3-c_~ }~yrene
Dibenz(a,h)anthracene
Benzo( g, h,i)perylene
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U ioou--
10U 100U
10 U 100 U
20 U 200 U
----
. -,-
--···--------10 U --. -·· .. 10 U
10 U
10 U
10 U
10 U
10 U
10 U -··-----·-··· 10 U
10 U
20 U
50 U 50U 500U -------·-·-··-_____ ,, ____ ----··-----------·-··-----------------.. ~=~~1----
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
20 U .
50 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
20 U
50 U Benzyl alcohol
Benzoic acid
Tot.ii cresoi 0.020 U 0.020 UJL 0.020 U 0.020 U 0.020 U 0.020 U ------------------·------------1------
Pyridine 0.020 U 0.020 UJL 0.020 U 0.020 U 0.020 U 0.020 U
Footnotes: -···-···· --·------·-----------1/ U code= analyte not detected at reported detection limit;
2/ UJL codes = €siim3ted qu·antitatioO iiffiit:·possibiS taise·ne98live dUe to ·out Oi contro1 surrogate-spike 01o·recovery;··(seie·page12-0i"r€POrt) ..
3i_~K _C?O~-~~--~ ~~~~-~i-~i~~~?_i_~~~j~~--~~~~atrix7nterrer~_~ce. see p~ge 13 Ct report-:----~-~-=~--=~=-~-----____ -___ ·_ ~:~.-:~-=-----=~-=-==:: _______ _
-' .. -..
Page 2
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-- --- - -- -- - -- -
Parameter/Sample ID
Acenaphthylene
Alachlor
Aldrin
Anthracene
Atrazine
Elliott
1.0 U
1.0 U
1.ou
1.0U
1.0 U
1.0 U
Table 4.4 Results of Analysis for OW Semivolatile Organic Compounds Using Method 525
Kubal-Furr and Associates
Stein Lambert
1.0U 1.0 U
1.0 U i 6 u
1.0 U 1.0 U
1.0U 1.0 U
1.0 U 1.0U
1.0U 1.0 U
Hoechst Celanese Semiannual GW Sampling
Martin
1.0 UJL i .6 ijji_
1.0 UJL
1.0 UJL
1.0 UJL
Walker
1.0 U
1.0U
1.0U
1.0U
1.0 U
Lab Blank
1.0 U
1.0 U
1.0U
1.0U
1.0U
1.0 IJJL i.0 U 1.0 U Benzo(a)anthracene ___ _ ------------------ ------------1.0 UJL 1.0 U ----i:o u··--Benzo(b }fluoranthene
f?enzo(k~!luor~nt_~ene ·
~er.zu(a)pyrene
~~nzo(g,h,i}~~~l~n~.
Butylbenzylphthalate
alpha-Ch_lo~~ane
~amma-Chlordane
! r~ns:n?pn.?~(1l?r
~-~hlor?biphenyl
Chrysene
Dibenz(a, h)anthracene
Oi--n-bUiY1Ptlihalate ----
2, 3-0ichlorobiptienyl
Diethylphthalale
·-· --
Bis ( 2-et_hyt~~~y ! ~~dip~!~_
Bis(2 -ethylhexyl)phlhalate
Dimethylphthalate
Endrin
Fluorene
~e~ta~~!?~ ....... _.
Heptachlor epoxide_._. _ -·-·
Heptachlorobiphenyl
He_x.iC:hi_of~~y~~~P1;rl~~~i~-~-e
lndeno( I,2,3-cd)pyrene
Undane
1.0 U 1.0 U 1.0U --------·-----------··--·----··--------·------<-----~
1.0 U
1.0 U
1.0 U Tau
1-0U
10U
1.0 iJ
1.0 u
1.0 U
1.0 U
10 u
1.0 iJ
1.0 U
1.0 U
1.0 U
1.0 U
1.0U
1.0 U 1.0 U 1.0 UJL · 1.0 U --··------. 1.0 U 1.0 U 1.0UJL 1.0U
1.0 U 1.0 U 1.0 UJL 1.0U --·--•---1.0 U 1.0 U 1.0 UJL 1.0 U
1-0U
1.0 U
1.0U
1.0U
1.0U
1-0U
1.0 U
1.0 U
1-0U
1.0U
1-0U
1.0 U
1.0 U
1.0 U
1.0U
1.0 U
1.0 UJL
1.0 UJL
1.0 UJL
1.0U 1.0UJL
1.0 U
1.0U
1.0U
1.0U
1.0 U 1.0 UJL 1.0 U
1.0 U 1.0 UJL .. ---· ----·····-1.0 U 1.0 UJL
1.0 v 1.0 uJL
1.0 U 1.0 UJL
1.0U 1.0UJL
1.0 U
1.0U
1.0 UJL
1.0 UJL
i _o iJ 1.0 i.JJL
i:ou 1.ou 1.0 U 1.0 UJL
1.0 U
1.0U
1.0 U
1.0 U
1.0 U
1.0 u
1.0U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0U
1.0 U
1.0 U
1.0U
1.0 U
1.0U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0U
LOU 1.0 U 1.0 U 1.0 UJL 1.0 U 1.0 U -------··-··--· -------
1.0 u , 1.-'-o ~u'------'----'1---'_o~u 1.0UJL 1.0U --i:Oi.J
1.0 UJL 1.0 U -1.0 iT . 1.0 U 1.0 U 1.0 U
1.0 U 1.0 U
1.0 U 1.0 U
1.0 U 1.0 U
i:oi.J 1.0U
1.0 U 1.0 UJL 1.0 U . -·-1.0 U
1.0U 1.0 UJL 1.0U
1.0U 1.0UJL 1.0U
.. ··-----·-·· ----· ·-···--···-·-----·-1.0 U 1.0 UJL 1.0 U
1.0U
1.0U
1.0U
1.0 U 1.0 U 1.0 UJL 1.0 U 1.0 U
---
~~thoXy~h!C!~
Octachlorobiphenyl
Pentachlorobiphe"nyt.
Pentactllorophenol
Phen.anthrerie · ·
(au ;:au 1.0 U 1.0 U
1.0UJL 1.0UJL 1.0UJL
1.0UJL 1.0U --·1.ou 1.0 UJL 1.0 uJi. -{o UJL ----·-------·-·----------,--~-, ----------------------
·-··----··---· ·····--·--· 1.0 U 1.0U 1.0U 1.0 UJL 1.0 U 1.0 U
Pyrene 1.0 U 1.0 U 1.0 U 1.0 UJL
Simazine 1.0 U 1.0 U "(() u·-· 1.0 UJL
1.0 U
1.0 U
1.0 U
1.0 U
T·e1ra.Ct11Cii-obipheny1 ···-1.0 u 1.0 u 1.0 u 1.0 uJL ·--fOTT·-· --·1 :ou·--···--·----·
Trichlol"obiphenyl . 1.0 U 1.0 U 1.0 U 1.0 UJL 1.0 U 1.0 U --·----------1----i--------·-· ·---------------
Footnotes: 1/ U code= analyte not detected at reported detection limit; 2i UJL =· 8.nalyte not detected ·at reported deteCtion limit; estirllated quantitation limit due to low surrogate spike recovery ot.itside control lilTiits (See page 15) and/or 0/odifterence on coritillUing ·c;·a1ibiatiOri-OUt ·of sPecifiCcliiOri-iof ·pe111achloropherlOT(Seepage--14):·----1·--·--------! . ---· --·--·-·1·--·-·------··1·--------·-··1 ·----.. --_::!_ ···--· -. ·-:(-·-----------1·· .. -· ·--.. ·· 1 ···
Page 1
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- --Kubal-Furr and Associates
Hoechst Celanese
Semiannual GW Sampling
-- -- -- - - -- ---Table 4.6 Results of Analysis for TAL / TCLP Metals in Groundwater and Sludge
SDG 3208 --------------------·---------------SDG 3195
Parameter/Sample ID FP TB238 TB247 ITEFF Lambert Martin Stein Walker OTEFF SBR SBR-TCLP TB239
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt.
~<:'~per
Iron
Lead
~agn~~i~m
~~nganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Footnotes:
---
83.5 U
3030 U
129 UJL
2.0 UJL
21.0U 3.0 UJL
13.6 U 12.3 UJL ---··-----·•--------,-c-=c.___1-
----------·-----1----1 1.0 UJI_
15 U
22.2 U
134 U
20.0 U
41.0 U
26.5 U ---·-----·-
5,720 JL
4.0 U 1.2 UJL
36.5 UJL
2.4 UJL
1,090 JL --------
21.0 U 1.0UJL
0.20 U 0.20 U
41.0 U
4.0 U
27,800 JL ------------
.. 2,310 JL ...
0.2 UJL
7.6 UJL
3,110 UJL
3.0 UJL
1.0 ULJ
523,000 UJL - -·--.... ··--3.0 UJL
1.0 UJL
15.5 UJL
1.6 U 5.5 U
J
-. -----. -------------------·· ·-----· """ ... ----···-·-·---·----~----·--·--··-------··
1/ U code= analyle not detecle~ at rep?~~?. d~t~~l)o~_lif!ii~ -. ... -· -... -
32.5 U 762 U
3.0 U 32.8 U
3.0 U 30.0 U 21.0 U
306 U
21.0 U
4.5 U
1.0 U 10.0 U ---f-----j----1·-'---'--------·----··---· 1.0 U 28.2 U 3.0 U 3.0 U
3.0 U
19, 000 ___ . ~}_1,_000
1.0 U 1.0U 73.8 U
----·----·--~!-U_ ··-6,130
1.0U
621
1.0 u
13.8 U
1,090,000
22.8 U
6,940 174,000 -------. ------------
4.0 U
21.0 U
_ -·---·-----· ----·-_ --~!_~. ·-1,630,000_
0.20 U
1.0U
6,770
3.0 U
1.0U
20.0 U
1,760
11~.~oo
20.0 U
30.0 U 41.0 U
18.0 U 4.0 U
.... 50, 100 __ .. 575,000 .
3.0 U
1.0 U
34.8
150 U ···1··· 10.0 U
447
-~--~-·--·-1-----+----I -·-----··--------------
4.0 U
43.9 U -
0.20 U
41.0 U
4.0 U
2/ JL code = estimated qua!1litali(:m (i~it, ~i~~~~-!~~; ~-~-~e!:: ~?I .P~?.P~r_ly ~~~~~~-~~ -~~~~ p-~~e -~? o_f -~ef:>~rt) __ --. ·----·----·----•-------· ··-·--·-.
3/ UJL code= analyte not delecled at reported detection limit; quantilalion limil estimated, possible false negative; sample not properly preserved (See page 17 or report).
Page 1
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- -- --- ----- --- -
Kubal-Furr and Associates
Hoechst Celanese
Semiannual GW Sampling
Table 4.6 Results of Analysis for TCL and TCLP Pestlcldes/PCBs Using Method 8080
Parameters/Sample ID
alpha.:BHC
beta-BHC
delta-BHC --. ··--~amm:8-~HC (Undane)
H~pt~chlor
Aldrin
~eP.~?~h!~!. ~poxid~ _
Endosulfan I
Dieldrin
4,4'-00E
Endrin
Endosulfan II
4_,4·-0~0
Endosulfan sulfate
4,4':00T
~et_hoxy<;:~!~r
Endrin ketone ---..... -~ndrin aldehyde
Chlordane
Toxaphf:.~~ .
Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Footnotes:
PB555
0.030 U
0.050 U
0.050 U
0.040 U
0.030 U
0.040 U
0.050 U
0.050 U
0.046 U
0.040 U
0.060 U
0.040 U
0.10 U . -----···-. 0.10 U o.io u ··--····-... 0.50 U
0.10 U
0.10 U
0.14 U1
5.0 U1
0.5 U1
o.5 ui
0.5 U1 ----- ---0.5 U1
0.5 U1
1.0 U1
1.0 U1
TCLP23B
0.25 U
0.25 U
0.25 U
0.5 U
2.5 U
5.0 U1
25 U1
FP
0.25 U
0.25 U
0.25 U
0.5 U
2.5 U ·-·-·· --·---
. ·---
5.0 U1
25 U1
1/ U code ::: analyte not detected at rePorted deieCtion liniii;
SBR (TCLP)
0.25 U
0.25 U
0.25 U
0.25 U
------------·. 2.5 U .. ·--------·-·
----------..
2.5 U1
5.0 U1
TCLP239
0.25 U
0.25 u
0.25 u
0.25 u
2.5 U
2.5 U1
5.0 U1
PB549
0.030 U
0.050 U - --------0.050 U
ITEFF
0.030 U ------··-. 0.050 U -----·-----· 0.050 U
0.040 U
0.030 U
0.040 U
0.050 U
OTEFF
0.030 U --· ------· 0.050 U ----------0.050 U
0.040 U
0.030 U
0.040 U
0.050 U
PB550 SBR
0.030 U 0.30 U -----. --0.050 U 0.50 U ------·-------0.050 U 0.50 UJL
0.040 U 0.40 U
0.030 U 0.30 U
0.040 U
0.050 U
0.40 U ------. -0.50 U
0040U
0.030 U
0.040 U
0.050 U
0.050 U
0.046 U
0.040 U
0.060 U
0.050 U 0.050 U 0.050 U 0.50 U
0.46 U
0.40 U
0.60 U
0.046 U 0.046 U 0.046 U - --------·-. 0.040 U 0.040 U 0.040 U
0.060 U 0.060 U 0.060 U
0.040 U 0.040 UJ 0.040 UJ 0.040 U 0.40 U
0.10 U 0.10U 0.10U .ffiou 1.0U ·-·-----·--· ----·--·---------------· 0.10 U 0.10 U 0.10 U 0.10 U 1.0 U
0.10 U 0.10 U 0.10 U 0.10 U 1.0 U ·--·--•-----------·-·· -·-----·--------------------·------0.50 U 0.50 U 0.50 U 0.50 U 5.0 U ---·---··-----------------------··------------------0.10 U
0.10 U
0.10 U
0.10 U
0.14 U1 0.14 U1
5.0 U1 5.0 U1
0.5 U1 0.5 U1
--------·-0.5 U1 0.5 U1 -·---------·-----0.5 U1 0.5 U1
0.5 U1 0.5 U1
0.5 U1
1.0 U1
0.5 U1 --------. 1.0 U1
0.10 U 0.10 U 1.0 U
0.10 U 0.10 U ------·------------0.14 U1
5.0 U1
0.5 U1
0.5 U1
0.14 U1
5.o ui ----------0.5 U1
0.5 U1
· 0.5 U1 0.5 Ui
1.0 U
0.14 U1
5.0 U1
5.0 U1 ---·--·-··-·· 5.0 U1
5.0 U1
0.5 U1 0.5 U1 5.0 U1
0.5 U1 0.5 U1 5.0 U1 -. ---·----·-----1.0 U1 1.0U1 ----· -· -··-·-----·-··--·-10 U1
10 U1 1.0 U1 1.0 U1 1.0 U1 1.0 U1
2, u1· coc1e· =··,;;naiyte·notdetecteCfai"reported dete-ction·1iffiiCCOmpound not Ca"iibratecnorTn·per·rorrr.-anceotmethO"d-by lab; (See pa9e 26i21):···-
3, UJL CO~E: ::: ~~a!v-ie ·n_o~ -~~ti~!~f ~~-~~~-i~~:~.:~~i~~~~~J\~~i_;~~~j~i~~~~.-~-~~~!tLa~~~-~~!~ _i~_f I~-~-f~!!_~~~J~~~·:p~~~~~~-~!-~"P._?_~1~:~-----~~:1 ~--··_-:
4/ UJ code::: anayte not detected at reported detection limit for %0 out of specification in continuing calibration (see page 21 of report).
Page 1
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. ·-.
- -- -- --- -- ----Kubal•Furr and Associates
Hoechst Celanese
Semiannual GW Sampling
Table 4.7 Results of Analysis For DW Pcsticides/PCBs In Groundwater Using Method 505
Parameters/Sample ID
Alachlor
Aldrin
Atrazine
Chlordane -....
Elliott
0.010 UQ1
0.010 U
0.010 UQ1 ... ---··--0.010 UQ2
Dieldrin 0.010 UJL
Endrin ii.Iii O i.i
Stein
0.010 UQ1
0.010 U ---·--0.010 UQ1 ------0.010 UQ2
0.010 UJL
0.010 U
Lambert
0.010 UQ1
0.010 U
0.010 UQ1 ----·-·-----0.010 UQ2
0.010 UJL
Ci01'cii..i --. --
Martin
0.010 UQ1
0.010 U
0.010 UQ1
0.010 UQ2 ..
0.010 UJL
0.010 U
Walker Blank
0.010 UQ1 0.010 UQ1 ----------·--··-· ·---·-----··---_____ ,. 0.010 U 0.010 U . - --· -----. ---·-· ---
0.010 UQ1 0.010 UQ1
0.010 UQ2 0.010 UQ2 -----0.010 UJL 0.010 UJL ., - -. --··· ··-· 0.010 U 0.010 U
--
Heptachlor 0.010 U 0.010 U 0.010 U .. Q,010 U _ 00 010 U 0.010 U .
Heptachlor epoxide. -·· -·--.J.:!l!~.Y.-:'~ __ _ll:_010_U_J~·--~:!Jici]:iL .. ~:!l!~_!:'J~ __ J.010_U_J'=.._ .... ~.01~__ll!l:_.I ___ ......j1 __ ...... _ .. ··---·· ····-.
Hexachlorobenzene 0.010 U 0.010 U 0.010 U 0.010 U 0.010 U 0.010 U
Hexachlorocyclopentadiene
Undane
Metho~ychlor
Simazine
-➔--·-------
"!"?..~.~pl~e~e
PCB 1016
PCB 1221
PCB 1232
PCB 1242
PCB 1248
PCB 1254
PCB 1260
Footnotes:
0.010 UJL
0010 U
0.010 U
0.010 UQ1
0.010 UQ2 ----0.010 UQ2
0.010 UQ2
0.010 UQ2
0.010 UQ2
-·-----0.010 UQ2
0.010 UQ2
. ,--.. ---·· ··-·· ---------· ------..... 0.010 UJL
0.010 U
0.010 U
0.010 UJL
0.010 U
0.010 U
0.010 UJL 0.010 UJL 0.010 UJL
0.010 U 0.010 U 0.010 U
0.010 U -.. --· --0.010 UQ1 0.010 UQ1 0.010 UQ1 -------------· ------------0.010 UQ2 0.010 UQ2 0.010 UQ2
0.010 UQ2 -- - --. ---0.010 UQ2
0.010 UQ2
0.010 UQ2 ---------·· 0.010 UQ2
0.010 UQ2
0.010 UQ2
0.010 UQ2 .. --------0.010 UQ2
---·-·------0.010 UQ2
0.010 UQ2
0.010 UQ2
0.010 UQ2 0.010 UQ2 --·· --------------------0.010 UQ2 0.010 UQ2 -----·------------· 0.010 UQ2 0.010 UQ2
0.010 U
0.010 UQ1
0.010 U . .. -·· --· ·-· . 0.010 UQ1
0.010 UQ2 0.010 UQ2
0.010 UQ2 0.010 UQ2
0.010 UQ2 0.010 UQ2
0.010 UQ2 0.010 UQ2
0.010 UQ2 --··---··· ··---0.010 UQ2
0.010 UQ2
0.010 UQ2
0.010 UQ2 --·-······-·--····--········ 0.010 UQ2
0.010 UQ2 0.010 UQ2 0.010 UQ2 0.010 UQ2 0.010 UQ2 0.010 UQ2
····-. -··· ...... -.. , ...... ..
-
1/ ~ co~e = a_1~~ly~~ !10!. ~~t':_c~e-~ al rep'?_r~-~~.~~t~~~i?.~ l~~i-~. _ _ __ ___ .. __ ·-·. __ --·-. -·-__ __ _ _ _ -•·--· _ ---· _______ -----· ____ ...... __ ___ _ -· _
2/ UJL code = analyte not detected at reported detection limit; quantitation limit estimated, possible false negative due to ¾RSD out of specification on initial calibration;
~~~eci1a~~dt
5:2
~e:~1~:P::•;~ ~o: ~elect~~·~~ ~e~~rt~-d-detectio~ ~i-~it; reSU1t~-~~tai~·~d ~Y-~~!~o~-~;~~---~~~-~~-~·ei~:~~~:65·-~-S~~~;:~~-~~~~; (S.ee ~a~~ 2512~ .. o; !~~o~;. I
4/ UQ2 code= analyte Was not n·ot dei"eCted at the reported detectioii liniit; fesults based entirely on chromatogram pattern; analyte no·t calibrated; laboratory technique
and methodology suspect; (See page 26) ·1-·--------i---··--·1 ···· ···-·--I -·-·· ·1 . I ·········1·-····--···-1•·••· . ·1
Page 1
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Attachment 5
Water-Level Measurements,
Water Sampling Logs, Chain-of-Custody Forms
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F
WATER SURFACE ELEVATIONS
Cleveland FACILITY Hoechst Celanese-Shelby, NC COUNTY
SIGNATURE _ _;C:,,;/_, ·~·.,._.._Q,,.1"",1c.<0..:(--"-----DA TE 3/6/95
WEATHER Overcast PAGE 1 OF 4
Measuring Depth to Water ~ Well Point Water Surface Remarks
dentification Elevation Surface Elevation
/feetl /feetl /feetl
A-39 823.36 9.91 813.45
B-34 790.62 13.32 777.30
C-49 864.11 13.94 850.17
D-27 845.50 16.35 829.15
D-35 845.69 16.84 828.85
D-58 845.19 16.67 828.52
D-88 845.52 16.94 828.58
F'-55 849.19 849.19 QED & Pulse Pum"-no w/I
G-50 848.48 46.43 802.05 No Lock
G--88 848.26 56.35 791.91 No Lock
H-59 845.25 50.70 794.55
H-79 846.53 53.68 792.85 No Cap
1-57 837.63 -30.47 807.16 Cut Lock-No Cap
J-28 825.18 20.22 804.96 Bailer in well
J-59 825.01 23.16 801.85 Bailer in well
K-28 811.20 11.94 799.26
K-58 811.39 14.03 797.36
M-28 806.72 30.66 776.06 Also Labeled as PZO-NN
M-44 806.71 29.39 777.32
N-29 803.38 8.21 795.17
N-53 803.82 10.70 793.12
0-25 807.54 13.75 793.79
0-59 806.61 12.30 794.31
Water levels were determined by use of a Solinst (Ontario, Canada) depth probe.
10 001
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WATER SURFACE ELEVATIONS
FACILITY Hoechst Celanese-Shelbv1 NC
SIGNATURE {/4.., Q;JiC 3/6/95
Cleveland
WEATHER Overcast
COUNTY
DATE
PAGE 2 OF _ __:4 __
Measuring Depth to Water
Well Point Water Surface Remarks
Identification Elevation Surface Elevation
ff eel) (feet) (feet)
P-31 790.00 25.10 764.90 Missing PVC Cao
P-58 788.12 26.59 761.53
Q-33 783.48 26.03 757.45 Missino PVC Cap
R-17 779.31 14.48 764.83
R-42 778.81 12.89 765.92
S-50 826.02 22.27 803.75 Lock Cut
,-.17 777.90 15.41 762.49
T-35 777.38 14.55 762.83
T-58 776.03 14.74 761.29
U-38 826.55 22.47 804.08
V-23 811.89 11.93 799.96
W-'23 800.91 18.20 782.71
X-32 796.96 17.40 779.56
Y-36 794.52 11.96 782.56 No Lock, Cover Ooen
y.74 794.87 12.34 782.53 No Lock, Cover Ooen
Z-78 797.08 24.15 772.93 PVC Cap Broken
AA-41 783.68 38.60 745.08 Drv· Hit top of Pump with Probe
AA-54 782.16 38.16 744.00
BB-18 771.75 6.91 764.84 Missing Cap
CC-33 812.68 22.10 790.58
CC-64 811.37 19.91 791.46
DD-58 796.10 34.74 761.36
EE-58 794.48 40.17 754.31
Water levels were determined by use of a Solinst (Ontario, Canada) depth probe.
10 002
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WATER SURFACE ELEVATIONS
FACILITY
SIGNATURE
WEATHER
G Well lentification
FF-23
FF-34
FF-62
GG-25
GG-39
GG-61
HH-48
HH-77
PZ-1
PZ-2
PZ-3
PZ-4
PZ-:SA
PZ-58
PZ-6A
PZ-613
PZ-7/.\
PZ-78
PZ-8
PZ-9
PZ-10
PZ-11
PZ-12
Hoechst Celanese-Shelby, NC COUNTY
(4:,, {'?J#, DATE
Cleveland
3/6/95
Overcast PAGE 3 OF 4
Measuring Depth to Water
Point Water Surface Remarks
Elevation Surface Elevation
/feet\ tfeet\ /feet\
772.33 13.36 758.97
772.73 13.87 758.86
772.19 17.98 754.21
771.64 21.05 750.59
770.44 20.22 750.22
771.78 21.81 749.97
755.44 38.64 716.80
755.87 38.43 717.44
773.99 19.30 754.69 Flush
795.81 37.90 757.91 Flush
786.62 33.67 752.95
750.07 3.60 746.47
788.72 36.63 752.09
777.59 37.98 739.61
795.11 44.03 751.08
796.89 44.91 751.98
780.46 29.00 751.46
784.46 9.65 774.81
767.99 7.76 760.23
788.96 35.45 753.51
784.65 46.10 738.55
805.48 58.81 746.67
749.41 0.35 749.06 No Can-W.L. at too of PVC casino
Water levels were detennined by use of a Solinst (Ontario, Canada) depth probe.
10 003
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FACILITY
SIGNATURE
WEATHER
[ Well dentification ·
PZ-13
OT-1
OT-2
OT-3
OT-4
0T-5
OT-6
OT-6A
OT-7
OT-7A
OT-8
IT-1
IT-2
IT-3
IT-4
IT-5
IT-6
IT-7
IT-8
IT-9
PEW-1
PEW-2
PEW-3
PEW-4
WATER SURFACE ELEVATIONS
Hoechst Celanese-Shelby, NC COUNTY
f'hJn ();,,jtli:,.,,_ DA TE
Cleveland
3/6/95
Overcast PAGE 4 OF 4
Measuring Depth to Water
Point Water Surface Remarks
. Elevation Surface Elevation
lfeetl lfeetl lfeen
776.51 21.42 755.09
774.36 15.91 758.45 Well Pumping
774.01 12.10 761.91 Well Pumoina
792.88 64.93 727.95 Well Pumoina
790.28 54.75 735.53 Well Pumpina
784.00 46.44 737.56 Well Pumoina
787.45 57.55 729.90 Well Pumoina
798.68 68.22 730.46 Well Pumpina
782.16 62.85 719.31 Well Pumpina
782.52 10.90 771.62 Well Not Pumpina
782.26 35.60 746.66 Well Pumpina
814.20 33.90 780.30 Well Pumping
813.85 37.80 776.05 Drv-No sounding-Well Pumpina
809.66 22.80 786.86 Well Pumoina
809.08 26.50 782.58 Well Pumpinq
810.64 23.10 787.54 Well Pumoina
812.20 34.80 777.40 Well Pumpino
27.00 -27.00 Well Pumoina
815.60 25.20 790.40 Well Pumpina
808.73 32.00 776.73 Not Pumoina
72.86 Well Pumoina-PVC to MP-0.80
85.98 Well Not Pumpina-PVC to MP-1 ,27
82.40 Well Pumoina-PVC to MP-1.38
81.95 Well Pumoina-PVC to MP-0.75
Water levels were determined by use of a Solinst (Ontario, Canada) depth probe.
10 004
,i ! E.i~pany
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GROUNDWATER FIELD SAMPUNG DATA SHEET
!EA, INC.
I.) Client Name: --1-Jlli"-'o"'-'e k'°<!h_,,,_s"'-'-f--'C.ue.<.Llald.<r1lL(w,\ce,_/; __________ _
2.) Client Location: Siie/6:f J NC
3.) Dale: ol (g I 'i'~ ----~~---
4.) Well ID Number --~fcc.cl_l ,_o-'-~~'---~--S.) Sampling Sequence II: -~D/ ___ _
6.) Sampler's Name: __ _,(.,.,. • ..,.,ha,...is._,__.d--"-vi: ....... IL.UA:(..,_~ _ll......=LIM~\)=½'1c.pd==.-----
7 .) Evacuatio,t Method: ___ Bailer
S.) Sampling Method: ___ Bailer
__ Airlift Pump
___ Bladder Pump
9.) Field Obse,:vations and Sampling Conditions
Outside Temperature: 7.-1 C'C)
___ Bladder Pump
ID Number ---
-.A.-~-Other
9.1)
9.2)
9.3)
Weather Conditions: Clear --1,_ Cloudy Calm __ Windy Rain
Was the well locked upon arrival? ___lL Yes
Any unusual conditions in the area? . Yes
If •y,:s• explain: . . Bt,s,Dlrllt '(]if 11..JM,
,YJ,,rr,t,h/ ---,,
j__NO
).-No 7i lo art;,,,,,-[. #Y
10.) · Well Evacuation (all measurements are referenced from the top of the well casing)
10.1) Casing Diameter (ID): ,\)A ___ (inches)
10.2) ToW Well ~th: A/A • ___ (feet)
10.3) Static Water Level: ,-)A • ___ (feet)
10.4) Height of Water Column: 'NA ___ (feet) (10.2 -10.3)
10.5) Water Volumo in Well: l\,}p. . ___ (Lit.ers/Gallons)
10.6) Evacuate 3 . t:82 Well -Volumes Prior to Sampling
10.7) Evacuate __ .,.. ___ (liters/Gallons) Prior to Sampling (10.6 • 10.5)
Tm<> Evacuation Started /(p : M (Use 24 Hour Time)
Trne Evacuation Completed I /e : 1? (Uso 24 Hour ~rne)
10.S) Actual Volume Evacuated {'/A • ___ (Liters/Gallons)
10.9) Did the well go dcy'I --~Yes )/ No
A) Time well went dry 1tflf : Date
B) Trne well was sampled I 1,,-_-:_/_S: Date?(-...,.,-, §.--S:---
C) Total time betweea evacuation and sampling ____________ (Hours)
11.) Groundwater Elevation
I 1. I) Surveyed Well Elevation (MSL) _______ (feet) Data Not Available
11.2) Static Wat,:;r Level NA (feet) ----
11.3) Static Water Elevation (MSL) ___ -____ ._ (feet)
d:\mi$c~frm\gmdwt.wp
10 005
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Well SamplinG Data
12. I) S.\lnplc Collected
Test Panm<:.tcrs Bottle Typo Siz.o Preservative Number Collected
D1,\ Sb.?. .z... \/1J 1io,Mi f(-c_, s
·1"'),.\ s-n~ ~ GJ,cc ),+ '-/ ·~ 2
·hCJ ,s2-s-(0(p.ss I~+-<fi>v 2-
12.3) Samplc: Appe:irance: . ?( Clear ___ Sediment Turbid ---
12.4) Samp!c,s placed on ice immediately after collection: ___lL Yes No
13.) Field Analyses
Parameter
Temperature ("C)
pH
Conductivity
(uS/cm)
Types of pH Buffers Used:
d:\misc-fcm\gmdwt. wp
Calibration Std.
N/A
4.C> /,.o .
I 15l>O
4.0
7.0
10.0
· Sample Reading
.. rz. cf
7,11-C
11°1
Lot Number -------LotNumber -------
Lot Number -------
Std. After Sample
NIA
7.DD
QC/,?
10
2
006
I Well ID Efl,oi+ 3
I C ·. 14.) Purge Summary
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Date & Time 3(r;/t( 3/ ;/ 'IS
I 1, tIIS 161S--
.
Volume Purged Lit. t1 ~cJ
Well Temp,,rature /Lf,5 /2,. lf
(°C)
Well pH Reading 7, )6 7AS
Conductivity 14_1 I J t./ (uS/cm)
Other
Remarks
15.) Well secured with lock after sampling? __i.o_ Yes No
16.) I, the undersigned, hereby certify that all of the above information is accurate.
Signature Date _ _,.3-1-[]..J,..J.l-'-'9.5""----
NOTE: Certs.in information (such as well elevations and mean sea level heights of well casings) cannot be
filled in on this form unless provided to IEA personnel by the client.
d:\misc•frm\gmdwt.wp
10 007
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1 t.l--\
M 11.quarion Company
GROUNDWATER FIELD SAMPUNG DATA SHEET
!EA, INC.
I.) Client Name: _,._,.//iJ.l.lf)~ ..... ,"-h=.s:..:...f__,,C...,.ecL.lla...,_11.wt...i..S:J.<.t __________ _
2.) Client Location: __ ..,.S.,_,Acue~lh"'-"l--l,(--IJ--'-'M'-'c.""---------------
1
3.) Date:
l
4.) Well ID Numbcr ___ S=---T-'--f"-'IN'-·-__,,----5.) Sampling Sequence//: __ ()~"]., ___ _
6.) Sampler's Name: ___ (,.....b....,a, ...... ·s _.d""'-"-'vr--'-'IAu.ii..,_~ __ --...,_I =µ.,...=-6 .... up"""P-'=d:-, ___ _
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7.) Evacuation. Method: ___ Bailer ---Airlift Pump ___ Bladder Pump
ID Number
,{ _ Other
8.) Sampling Method: ___ Bailer ___ Bladder Pump ---
9.) Field Obser,ations and Sampling Conditions
Out.side Temperature: __ .... J......,_{ ___ (."C) 9.1)
9.2)
9.3)
Wcath:r Conditions: Clear _X_ Cloudy Calm __ Wmdy Rain
Yes _L_No
Was th.e well locked upon arrival?
Any unusual conditi_ofe _the area?
If "Yes" explain:· · 1Dws:,.l ·.
---:::-"-r. Yes No
i.0w, 0d: euac-.,,/ 91 [)) er;,~ w, tu -1--{, 1t-.<
. 0 ,
10.) · Well Evaeuatio.~ (all measurements = refere.nced from the top of tho well easing)
10.1) Casing Diameter (ID): .J 1\-• ___ (mches)
10.2) Total Well Depth: ~----(feet)
10.3) Static W,w Level: -ld..!l_ . .,..-__ (feet)
10.4) Height of Waler Coln= I )'l\ ___ (feet) (10.2 -10.3)
10.5) Waler Volume in Well: Alf,-• ___ (Liters/Gallons)
10.6) Evacuate 3 . ® Well Volumes Prior to Sampling
10.7) Evacuate __ _...:• ___ (llters/Gallons) Prior to Sampling (10.6 "' 10.5)
T'une E·raeuation Started / lo : 30 (Use 24 Hour Time)
T'unc Bvai:uation Completed /lo : @ (Use 24 Hour Time)
10.8) Actual Volume Evacuated !~111, • ___ (Liters/Gallons)
10.9) Did the well go dxy? ---,,.,-Yes ~--No
A) Timc well went dry l}~: Date
B) Time well was sampled l&-.-,-Y-o Date -1-+fz,--fr.qc-i',----
' I
C) Total time between evacuation and sampling ___________ (Hours)
11.) Groundwater Elevation
I I. I) Surveyed Wei! Elevation ~SL) _______ (feet) Data Not Available ___ _
11.2) Static Water Level /Jr\ (feet)
I 1.3) Static Water Elevation (MSL) _________ (feet)
·l 0 008
I Well ID 5fe1Af
Well Sampling Data I/
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12.1) Sample Collected
Test Para.m.e,~ern Bottlo Typo
¼'i r;,1)7,. 7,, Vlllv
l)[N 5D5 0~
])t,J 5i5 61o-v
<t J-.4-D v1iJ
f,... loO/D //,,,/If
,oc v i cJI
2
Siz.e Preservative Number Collected
Lj O .,JI tf<_{ 3
OJ ~t 2
0 ,f q.t 2-
Lf 1 ,.,J ~{( 3
5/rri Li I\ Ji'>? )
40..J 41 Sol{ "2-
I 12.3) Sample Appearance: )( Clear __ Sediment Turbid
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12.4) Samples placed 011 ice immediately after collection: ...x._ Yes --No
13.) Field Analyses
. -Parameter
Temperature (°C)
pH
Conductivity
(uS/cm)
Types of pH Buffers Used:
d:\misc-frm\gmdwt.wp
Calibration Std.
NIA
4.C> f 1,D .
IIZD
4.0
7.0
10.0
Sample Reading
'' (7, 2,
1-l-7
c;~
Lot Number ------Lot Number ------Lot Number ------
Std. After Sample
NIA
7 01)
Cftg
10 009
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(_
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14.) Purge Summary
Dale & Time 3/fa/c;r i/6/?5
/&;,Qf{; 16l/G
Volume Purged vt+. /~J
Well Temperature 17.0 I?,< ("C}
Well pH Reading 7.2~ f],}__')
Conductivity 53 53
(uS/cm)
Other
Remarks
.
15.) Well sccurcd with lock after sampling? i Yes No
16.) I, the undersign,,d, hereby certify that all of the above information is accurate.
I] f)
Signature _j__ < ~ ~rA Mlv--Date_3:..+/4c:...it/4~s::::: __ _
N01B: ~rtain infonnation (such as well elevations and mean sea level heights of well casings) cannot bo
filled in on this form unless provided to lEA personnel by the client.
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10 010
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M ,'.qua,ion company
GROUNDWATER FIELD SAMPLING DATA SHEET
!EA, INC.
1.) Client Name: _.,_tfi~o=C-C-~h=.s_f_C,=ela~t1~f~-S:-t ____________ _
2.) Client Location: __ -S._.b-R~/h~11,_..
1
~N!~L-_____________ _
3.) Date: _3/ {g PS' '1
4.) Well ID Number ___ /J)_,nWir ___ · --=----5.) Sampling Sequenco #: --~0_· ""] __ _
6.) Sampler's Name: ----1C.,....h1-UR ..... is._O,.,.__,._vf ...... le ...... r.,_;') __ Ji_-->-=J.A,v-..==--_,_6..,..Aq.,yr,,...,.-;;i="-----
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7.) Evacuati.on Method: ___ Bailer ___ Airlift Pwnp
___ Bladder Pwnp
___ Bladder Pwnp
ID Number
Other --~
8.) Samplin1: Method: ___ Bailer ---
9.) Field Observations and Sampling Conditions
9.1) Outside Temperature: --~*'--!'----(."C)
Wc:ather Conditions: Clear ____,.\L Cloudy Calm __ W"mdy Rain
9.2) Was the well locked upon arrival? Yes .x:__ No
9.3) Any unusual conditiow in '!ir area? .....(k. Yes No , / / ,, ,,,/Lil
If 'Yes' explain: _.,t'l/4t=ao""m""""'""&""~-'-'-:---',;l.<l .... <.><....,4.,.1 ... &......,.p"'-'-....P.,"-,,f'-l{J>"'l"'-:; .. µ.,.;ft=c1C-.j.'tN.L.l<, .. '4c ... J.,.Y""""ll;,c:_h~,i,"''.,'..,,_:t
10.) ·Well Evacuation (all measurements are referenced from the top of the well casing)
10.1) Casing Diameter (ID~: . ___ (mches)
10.2) Tobll Well Depth: • (feet)
10.3) . Static Wmr Level: . (feet)
10.4) Height of Wmr Colwnn: I.JG • ___ (feet) (10.2 -10.'.l)
10.S) WaJ;,r Volume in Well: »M . ___ (I.itecs/Gallons)
10.6) Evacuate 3 . pp Well -Volumes Prior to Sampling
10.7) Evacuate ~ l)A: . ___ (liters/Gallons) Prior to Sampling (10.6 * 10.S)
Time Evai:uation Started {lo : l{: S:: (Use 24 Hour Time)
Time Evacuation Completed / (q : S::f (Uso 24 Hour Time)
10.8) Actuttl. Volume Evacuated IV-' ·-,-.---(I.iters/Galloos)
10.9) Did the well go d,y'! __ ~Yes (,£ No
A) Time well went dry ,iJA : Date
B) Tune well was sampled-/ (o-. :-5-i;; Date -3-,/-1o-r/q-s-=---
C) Totill. time l>etw=i evacuation and sampling ___________ (Hours)
I I.) Groundwater Elevation
I I. I) Surveyed Well Elevation (MSL) _______ (feet) Data Not Available
11.2) Static Water Level ,\M (feet) ----
11.3) Static Water Elevation (MSL) ___ -_____ (fect)
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12.) Well S.1mpli

□

g

Data
12.1) Sample C<>llected
Test Parameters Bottle Typo
"JDC... viJ
<;oz_. 1-bw \J,cJ.
c;oc; llc.!';Oo,-.4
5 z.s-616..<J,J
Sit.e
4o..J
(1)\ -0
1 i J ,
{};f:
Preservative Number Collected
+l,SC11 ;?
Jc1 3
</~ ::2
'f 'l ;2
'
12.3) Sample Appearance: '('.__ Clear ___ Sediment Turbid ---
12.4) Sam,ples placed 011 ice immediately after eollcction.: __2{__ Yes No
13.) Field Allaly,:es
Paramet<~
Temperature ('C)
pH
Conductivity
(uS/cm)
Types of pH Buffers Used:
d:\misc~frm\gmdwt.wp
Calibration Std.
NIA
i-/-.C> /-, .(>
'
l15oD
4.0
7.0
10.0
Sample Reading
Ii l I
7,7,Z,,
ZS-3
Lot Number -------Lot Number -------Lot Number -------
Std. Aft.er Sample
NIA
1.111)
Cf\C\
10
2
012
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Well ID
14.) Purge .Summary
Date & Time 3/te 19 <;' 5'/b/c,s
II.Pt/5 Jt,,~<;
.
Volume Purged J:j-Jt. M+v
Well Temperature /0, S rt( (-CJ
Well pH Reading 'l, I~ '7, 22-.
Conductivity JJ{9 2SJ (uS/cm)
Other
Remarlrn
15.) Well secured with lock after sampling? _{_ Yes No
16.) I, the undersi1;ned, hereby certify that all of the above information is accurate.
NOTE: Certain information (such as well elevations and mean sea level heights of well casings) ·cannot be
filled in on this form unless provided to IEA personnel by the clienL
d:\misc-frm\gmdwt.wp
10
3
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l .C.L-\.
M Aquaricn Company
GROUNDWATER FIELD SAMPLING DATA SHEIIT
!EA, INC.
L.) Client Name: _ _,_U.,.fl"e'-'c....,h_,.,.s"-f'---"'0'--"e'-'-'la"'"rz~(, .... {,€~-------------
2.) Client Location: __ ...,,1.\"'--b..,,P...,_/2=~.:,-Lf.....,1>----'-N('-e,~--------------
3.) Date:
l
Jµc1&{~,f
'M ✓
4.) Well lD Number -~Uf.....,.~-------5.) Sampling Sequence II: --=c'.J'--'t'-----
6.) Sampler's Name: ---'=,C,.µho ..... i.s'-'d'""--"-'-vt-il.lla-w_....,]..,..1%-,,~8»t~-d"""'-----
7,) Evacuation Method: ___ Bailer -----,-Airlift Pump
___ Bladder Pump
___ Bladder Pump
___ ID Number
8.) Samplb,g Method: ___ Bailer
9.) Field Observations and Sampling Conditions
9.1)
9.2)
9.3)
Outside Temperature: Z f ("C)
Weather Conditions: Clear _>(_ Cloudy Calm _ Wmdy
Was the well locked upon arrival? Yes X No
Anyunusual"':'nditi.onsw~;=? _ 4't_es y~oL 1 -~ ~
If 'Yes' cxplam! . ~~, ~ ~ if IQ ®~1
_,,<?~ . .
10.) ·well Evru=tion (all measurements are referenced from the top of tho well casing)
10.1> easing Diameter (ID): tJA . __ (inches>
10.2) Total Well Depth= (1;'.A • __ (foet)
10.3) Static Water Level: .'~ lJ •-re-_ (feet)
10.4) He\ght of Water Column: ~ • ___ (feet) (10.2 -10.3)
10.5) Water Volume in Well: ,WI: • ___ (liters/Gallons)
10.6) Ev•.cuate 3 . t@ Well Volumes Prior to Sampling
10.7) Evacuate UA . ___ .(Liters/Galloir Prior tci Sampling (10.6 * 10.5)
Time Evacuation Stam<! (1 : (Use 24 Hour Tune)
Tlllle Evacuation Completed J-1 : IO (Uae 24 Hour Timo)
10.8) Actital Volume Evacualed µ.A . ___ (liters/Gallons)
10.9) Did the well go dry? __ ,_Yes ~"---No
A) Tune well went dcy jJ. :___ Date
B) Tune well was sampled /1. :_iv__ Date:, -z--r4"c-/o+,~-,S::,----
C) Total time between evacuation and sampling ______ ,_1 ____ (Hours)
11.) Groundwater Elevation
II.I) Surveyed Well Elevation (MSL) _______ (feet) Data Not Available_-::_-:: __
11.2) Static Water Level /Wr (feet)
11.3) Static Water Elevation (MSL) ________ ._(feet)
d:\misc•frm\gmdwt.wp
10
Rain
014
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u
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••
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12.) Well Sampling Da~,
12.1) Sample Collected
Test Parameters Bottle Typo
'jl)'._. \),r.
<oz..z. t-J \J\cJ
~DC: i)i..) r::o ,,A A
{;71>-') l)W r;~
Size
!./Q,,.f
t/o.J
!J .I
():/
2
Prescrvati vc Number Collected
!-I So,1 ;2.
itct , 3
l/9 )-
i!0 ;2
12.3) Sample Appearan= . ~ Clear __ Sediment Turbid ---
12.4) Samples pla=l on ice immediately after collection: JL_ Yes No
13.) Field Analyses
l'arameter
Temperature ('C)
pH
Conductivity
(uS/cm)
. Types of pH Buffers Used:
d:\mise•frm\gmdwt. wp
Calibration Std.
NIA
4.6 f,.D .
l15lm
4.0
7.0
10.0
Sample Reading
/)1f
(p ,'it/
WI
Lot Number -------Lot Number -------Lot Number -------
Std. After Sample
N/A
/,61-,
%
10 015
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Well ID _-_,_M-\-Ucr;;Jt,.,,.,.,,""' "--"'--' _
\
14.) Purge Summary
Date & Time ?J~/qr-
/7cm
Volume Purged v+.
Well Temp,,rature (}.? (·C)
Well pH Reading G .i&
Conductivity l-/44 (uS/cm)
Other
Remarks
"3/lof~
n/0
Ak<r
/>,g
b, 'tl/
4 ~ I
15.) Well secured with lock after sampling?__!:,_ Yes No
16.) I, the undersigned, hereby certify that all of the above information is accurate.
Signature--'=('-"-'' L~U""-L<u'-"'-"M-="-"-=----
'
NOTE: Certain info.rmation (such as well elevations and mean sea level heights of well casings) cannot be
filled in on this form unless provided to IEA personnel by the clienL
I d:\misc-frm\gmdwt.wp
I
I 10
3
016
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iti-\.
AA A.(luorion Company
GROUNDWATER FIELD SAMPUNG DATA SHEET
!EA, INC.
I.) Client Name: _..._!-/4,..D=e ..... c'-'--h=cS'-'-f--'0'"'-e....,laCld..L.au.e ..... S..,_t ____________ _
3.) Date:
2.) Client Location; SAe/61,( J NC
:3/ & (q<:: '1
4.) Well ID Numbcr _-/JJ~oJk~~~---::---5.) S~ Sequence II: --0~£~---
6.) Samp!Cl"'s Name: __ ....,.(,....,ho ...... is._O~trt ......... la'-"",~-----Z,;.,__,~~1-6-...-;dfr""'l'.ul ..... i ....... , ---
l
7.) Evacuation Method: ___ Bailer ___ Airlift Pump
___ Bladder Pump
___ Bladder Pump
___ ID Number
Other --~
8.) Sampling Method: ___ Bailer
9.) Field Ob,sctVations and Sampling Conditions
Outside Temperature: ______ ("C)
9.1)
9.2)
9.3)
Weather Conditions: Clear __ Cloudy Calm __ Wmdy Rain
Wa., the well locked upon arrival? Yes No
Anyunusualconditions~. __ Yr:,; ~No . ;/
If "Yes" explain: . .~ ' I~ <n .%!:!:::5_ ,1,<.M.<--~
~
10.) ·well Evacuation (all measurements arc referenced from the top of tho well casing)
10.1) Casing Diameter (ID): lµc . ___ ('mchr:,;)
10.2) Total Well Depth;~-. __ (feet)
10.3) Statfo WaJ.er Level: _;!M_. ___ (feet)
10.4) Height of WaJ.er Column: ,M<l . ___ (feet) (10.2 -10.3)
10.5) Wate.r Volume in Well: ,,v.4 . ___ (liters/Gallons)
10.6) Evacitatc 3 . @ Well Volumes Prior to Sampling
10. 7) Evacuate 1/'A: • ___ (Litcrn/Gallons) Prior to Sampling (10.6 * 10.S)
Tune Evacuation Started ~0_: 1 :;--(Use 24 Hour Timo)
Tm1e Evacuation Compl~J : ~ (Use 24 Hour Timo)
10.8) Actual Volume Evacuated wf..-. ___ (liters/Gallons)
10.9) Did tho well go d,y'l ___ 'Yes t--No
A) Tim<> well went dry 1JJ. '---:-c Date -;--,-,----
B) Tune well was sampled .-p!l: J,<; Datc __ i,('r-"'-wt-(K~--
C) Total time between evacuation and sampling ___________ (Hours)
11.) Groundwater Elevation
1 I. 1) Surveyed Well Elevation (MSL) _______ (feet) Data Not Available_-::_-=. __
11.2) Static Walt!r Level _-"gl....,/;j..__ ___ (feet)
11.3) Static Water Elevation (MSL) ___ -_____ (feet)
d;\misc•fnn\gmdwt.wp
10 017
12.) Well Sampling DaL,
12. I) Sample Collected
Test Para.meters Bottle Typo Siz.c Preservative Number Collected
1Dl 1/tcJ '10..l 1-1, <o,; ,J.,
r;oz..2-1)(,J VlcJ. fo...0 HC( 3
50( DW fiO. ,A 2:J Y'l ;;.
Sis-"Dw r10,,,~ O;i ifv :).,-
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I 12.3) Sample Appearan~: _.,.___aear ___ Sediment Turbid ---
12.4) Samples placed on i~ immediately after collection: _X._ Yes No
I 13.) Field Analy:;es
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Paramet~
Temperature (°C)
pH
Conductivity
(uS/cm)
Types of pH Buffers Used:
d:\mise.frm\gmdwt.wp
Calibration Std.
NIA
4.1) /,.o .
ICiZSD
4.0
7.0
Saniple Reading
17, 1./
/, 1'7
6?
Lot Number -------Lot Number -------
10.0 Lot Number -------
Std. After Sample
N/A
7-D'D
°lfi
10
2
018
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WelllD-W~
t
'-· 14.) Purge Summary
Dale & Time 3/~R" '3/ t,,'(<S--
n-i.o l I ~.,;
Volume Purged Jj,Jt. Afi-e-
Well Temperature !7,b 17,1 . ("C)
Well pH R,:,ading 7,0~ ?.17
Conductivity 2DD 1~i (uS/cm)
Other
Remarks
15.) Well secured with lock after sampling1 ~ Yes No
16.) I, the undersigned, hereby certify that all of the above information is accurate.
Signature _ _,_.{L~~!J-"---Lz!Jfa-'-<M---___ _
NOTE: Certain infllrmation (such as well elevations and mean sea level heights of well casings) cannot be
filled in on this form unless provided to IBA personnel by the client.
d:\mise-frm\gmdwt.wp
10
3
019
.~ !~!c~, l
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I.)
2.)
3.)
Client Name:
GROUNDWATER F!EU) SAMPUNG DATA SHEET
!EA, INC.
//o~chsf Cela11t5t
Client .L=tion: SJe/4! ' All
::it,1hs-Date: I
4.) Well JD Number T)-35 5.) Sampling Sequence #: --~D~l, __ _
6.) Sampler's Name: C.bQi.s dirtlaw -;-Mn fwtwd
7.) Evacuation Method: ___ Bailer ___ Airlift Pump
___ Bladder Pump
___ Bladder Pump
ID Number
X . Other
8.) Sampling Method: ___ Bailer
9.) Field Observations and Sampling Conditions
9.1)
9.2)
9.3)
Or1tside Telllf>Ctalllre: ___ .._/ ~/p __ ("C)
Weather Conditions: Clear _L Cloudy
Was the well locked upon arrival?
Any unusual conditions in the area?
___i... Yes
Yes
---
Calm
No
~No
__ Wmdy
If 'Yes' explain: _______________________
_
10.) · Well Evai:uation (all measu=ents are refe:cneed from the top of tho well casing)
10.1) Casing Diamcicr (ID): J, . OD (mches)
10.2) Tc,tal Well Depth: 3 5 . cm (feet)
10.3) Sbltic Watu Level: I le • ~ f (feet)
10.4) Height of Water Column: I~ .__lL_ (feet)sl • 10.3)
10.5) Wu.tor Volume, in Well: J., • ~ten,/ allons
10.6) Eva.cuato ±· t8) Well Vol Prior to ling
10. 7) Ev.ocuate • /'JD (U · G onsJ frlor to Sampling (10.6 "' 10.5)
'Time Evacuation Started -"'--"-~:.,....."'<;"""= (Use 24 Hour Time)
Tune Evacuation Completod,,-_.,..~: 0 (Uso~our Time,)
10.8) Actual Volume Evacuated -~-·_m__ (litors/~)
10.9) Did the well go city? _ _,..,,_Yes_-__,--..,__~ No
A) Time well went d,y ~/Pr :~--Dato
B) Time well was sampled 0~: GO Dato _:=3;)_...1:1~9:,'5'.J.. _____ _
C) Total time between evacuation and sampling ___________ (Hours)
11.) Groundwate:r Elevation
11.1) Surveyed Well Elevation (MSL) -,-------(feet) Data Not Available -
11.2) Static Wat,;r Level ( ~ , I{~ (feet)
11.3) Static Wat,;r Elevation (MSL) ___ -_____ (feet)
d :\misc•frm\grndwt.wp
Rain
10 020
I Well ID
12.) Well S,mpling Da~,
I 12.1) .Sample Collected
Test Para.meters Bottle Typo Size Preservative Number Collected
/!'JC V1i:J! 40 ,,, 0 fl½, 3
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12.3) Sample Appear.moo: . X Clear ___ Sediment Turbid ---
12.4) Samples placed on ice immcdiatoly aftet-collcction: ~ Yes No
13.) Field Analy::es
Parameter
Temperature (°C)
pH
Conductivity
(uS/cm)
Types of pH Buffers Used:
I d:\mise4 frm\gmdwt.wp
I
I
Calibration Std.
NIA
'-t.C> f,.D
'
I l5l5r>
4.0
7.0
10.0
Sample Reading
,q, /.-
4.t/7
it/~
Lot Number -------LotNumber -------Lot Number -------
Std. After Sample
N/A
w,qq
~qq
10
2
021
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Well ID D-3s
14.) Purge Summary
Date & Time 5/7/q~ 3/1 rs
n9.L( 0'35(3 .
Volume Purged r.,.i-1-. 3 lo 9c.10 Al:h.,.
' ' V
Well Temperature 11.0 /1.& Io/ I~ /~-2-Ii, I
(°C)
Well pH Reading S-)~ t-/,1! '-/, ZC1 4,i7 4,13
Conductivity IS 3 ISi (41 ,q, /50 (uS/cm)
Other
Remarks
·. \ 15.) Well ~ with lock after sampling?~ Yes No
16.) I, the undersigned, hereby certify that all of the above information is accurate.
Signature -----I--'-( h~/)M -1-,'(J~IJl}Ok-=----
NOTE: Certain information (such as well elevations and mean sea level heights of well casings) cannot bo
filled in 011 this form unless provided to IBA personnel by the client.
d:\misc-fcm\gmdwt.wp
3
10 022
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M AQur,rion Company
I.)
2.)
3.)
4.)
6.)
Client Name:
Client Location:
GROUNDWATER FIELD SAMPLING DATA SHEET
!EA, INC.
l-loe ens f Celaat~t
t/C SAe/6;!/,
Date: 3i7h.~ I
Well ID Number 1) -,S~ 5.) aling Sequence /I:
Sampler's Name: C.bo,s Ovl:la,;) %m 13qo4
1
07
7.) Evacuation Method: ___ Bailer __ Airlift Pump
___ Bladder Pump
___ Bladder Pump
ID Number
~X-~. Other
8.) Sampling Method: ___ Bailer ---
9.) Field Ohservations and Sampling Conditions
9.1) Outside Temperature: /._8' (."q
W cather Conditions: Clear ~loudy --Calm __ Wmdy Rain
9.2) Was the well lockc:d upon arrival? Yes No
9.3) Any unusual conditions in the area7 Yes -t-No
If "Yes' explain:
10.) Well Evacuation (all measurements are referenced from the top of the well casing)
10.1) CasiJO.g Diameter (ID): 1-. . (JD (mches)
10.2) Total Well Depth: 5lo 1.0 (feet)
10.3) Stati.c Water Level: / lo . -1, 1 Jr) .
10.4) Height of Ww.r Column: "f! . (feet)el0 -10.3)
10.5) Watt.,r Volwno in Well: lo . (llters/ <i ·
,o.~ "'""" 3 . @ W<ll •~7 • m,
10. 7) Evacuate '.2. 0 • C)Q (llters/ o Prior tci Sampling (10.6 • 10.5)
Time Evacuation Started D8 : (Use 24 Hour Time)
Time Evacuation Completed OJ : "2-(U"'.' J.H:<?ur Timo)
10.8) Acturu Volume Evacuated 1 D • (JO (llters/G~
10.9) Did the well go dxy7 Yes :X No ·
A) Time well went d,y ~: Date
B) Time well wa.s sampweq..-_-,--=:z_--,~ Date _:::_:3:/-"1...,_ "f".1--(q~?~:::_:::_-
q Tout! time between evacuation and sampling ___________ (Hours)
I I.) Groundwater Elevation
11.1) Surveyed Well Elevation (MSL) _______ (fcet) Data Not Available_-:_:: __
11.2) Static Water Level (~.~ 7 (feet)
11.3) Static Water Elevation (MSL) ________ ._(fect)
d:\misc~frm\gmdwt.wp
10 023
l2.) Well Sampling Data
l2. l) Sample Collected
Test Panuneters Bottle Typo Size Preservative Number Collected
-nv/ \) /Q (/ Cfi),Nl\Q H, Slh, )_
.
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I 12.3) Sample Appearance: c Clear ___ Sediment Turbid ---
12.4) San,ples placed on ice immediately aft<:r collection: ---2\_ Yes No
I 13.) Field Analyses
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Parameter
Temperature (°C)
pH
Conductivity
(uS/cm)
Types of pH .Buffers Used:
d:\mise•fcm\gmdwt.wp
Calibration Std.
NIA
4--C> f,-D .
1 "757"',
4.0
7.0
10.0
· S-aniple Reading
)9, z.
5.S-7
3/p
Lot Number ______ _
Lot Number -------Lot Number -------
Std. After Sample
NIA
lo_qq
qqq
10
2
024
••
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Well ID
i ' ·-"l4.) Purge Summary
Dale & Time 3/1fif
cR'i'<
Volume_ Purged L,Lt. 1 )4
Well Temperature /~. 7 ;t,5 /?!I (°C)
Well pH Reading s.~~ S,39 5:61
Conductivity ?~ ]5 37 (uS/cm)
Other
Remarks
15.) Well secured with lock after sampling? _j_ Yes
3
"?/1/cis
01L,; .
w~aO AWA
(, ' l)
(i,2-_ /Y,:?.
5,57 5,5{
35 35
No
I 16.) I, the undersigned, hereby certify that all of the above information is accurate.
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NOTE: Certain information (such as well elevations and mean sea level heights of well casings) cannot be
filled in on this form unless provided to IEA personnel by the clienL
d:\mise-fnn\gmdwt.wp
10 025
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l Lll)..
An AQua,ion •:Ompany
GROUNDWATER F!El.D SAMPLING DATA SHEET
!EA, INC.
I.) Client Name: (-/De e,h.s f Ce. la 11 !SE
2.) Client Location: S!ie/6 u , NC
3.) Date: '37/7 tQ 5:. ,{
4.) Well ID Number 5.) Sampling Sequcneo #: Q-23
6.) Sampler's Name: C bols dvl:law k &10/it
7.) Evacuati,,n Method: -~K_Bailer
8.) Sampling Method! _ ____c'f-_Bailer
--.,-Airlift Pump
___ Bladder Pump
___ Bladder Pump
___ ID Number
1
a~
Other --~
I 9.) Field Observations and Sampling Conditions
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9.1) Outside Temperature: ___ 2:~0~ __ ("C)
We:1ther Conditions: Cleor _J._ Cloudy
9.2) Wa,; the well locked upon arrival?
9 .3) Any unusual conditions in the area?
__x_Ycs
Ye:,
__ Wfody Rain
If 'Ycs' explain: --,---------------------,---
10.) Well Evacu:ition (all m=cnts are referenced from the top of tho well casing)
10.1) Casing Diameter (ID): :Z, . W (mchcs)
10.2) Total Well Depth.: 2-9 . v7> (feet)
10.3) · Static: Water Level: 2,0 . 2, 1-(feet)
10.4) Height of Water Column: ?' . J 8 -~) (10.2 -10.3)
10.5) Wau,, Volume in Woll: 5 . iJ '--(T@&/Gallom)
10.6) Evaci:tato 3 . @ Well Volume:, Prior to Sampling
10. 7) Evac\late / 7 . {Jl) ~Gallom) ,Prior to Sampling (10.6 " 10.5)
Ttr.llo Evacuation Started QC,-: (5 (Use 24 Hour Tune)
Tw1e Evacuation Completed IO : I ()_({Jso 24 Hour Tune)
10.8) Actual Volume Evacuated (-i ._{jQ_ ~allons)
10.9) Did th,, well go d,:y? _~~Ycs ___{_No
A) Tun<: well went dry A/iA: :___ Dato
B) Tune well was sampled (/\-( Q Dato -3~(-1 +-8-.,----
C) Total time between evacuation and sampling 1 (Ho=)
I I.) Groundwater Elevation
1 !. l) Surveyed Well Elevation (MSL) ______ (feet) Data Not Available ___ _
I 1.2) Static Water Level 1-0, Z. 2 (feet)
11.3) Static Water Elevation (MSL) ___ -____ (feet)
d:\mi$c•frm\gmdwt. wp
10 026
Well ID 2
12.) Well Sampling DalA
12. l) Sample Collected
Test Parameters Bottlo' ypo Size Preservative Number Collected
wv 1)111 wovrJ r11 sot} d--
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I 12.3) Sample Appearance: . X Clear ___ Sediment Turbid
12.4) Samples placed on ice immediately after eollcction: ...i__ Yes ---No
I 13.) Field Analyse,:
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Parameter
Temperature ('C)
pH
Conductivity
(uS/cm)
T)'pcs of pH Buffors Used:
d:\mis<>(cm\gmdwt.wp
.
Calibration Std.
N/A
i.f-.C> /-, -0 .
I ,sm--,
4.0
7.0
10.0
Sample Rea.ding
11-~
1,,30
xt./0
Lot Number ______ _
Lot Number -------Lot Number -------
Std. After Sample
N/A
/,,, CA
_, -., ,.,,,,.. (Cm
.;-,-v"' "
10 027
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Well ID ~~'--.ch'-"q __ _ 3
14.) Purge Summary
3-'7-'7 ~ 3(17qs-Dale & Time .
'1: ,;-s-lb ,o
Volume Purged J:,,Jt. (9 11-11QJ A~
V
Well Temp<:rature I'. e, / 9;_ I /7.7 /7. 't 1.7.</ (·C)
Well pH Reading C,.32-c,.J'=, 0.J}f t.Jb G,:) 7
Conductivity i,_;, .iJ7 '6 ~z <?;<+9 <t;G.D (uS/cm)
Other .
~FIJ_?
.
Remark;;
15.) Well secured with lock after sampling? _j_ Yes No
16.) I, the undersigned, hereby certify that all of the above information is accurate.
Date_....::{)_:J..:..0.:....7.,_9.,_5 ___ _
NOTE: Certain information (such as well elevations and mean sea level heights of well casings) cannot bo
filled in on this form unless provided to IBA personnel by the c!ienL
d:\misc•frm\gmdwt.wp
10 028
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GROUNDWATER FIELD SAMPUNG DATA SHEET
!EA, INC.
I.) Client Name: _ _.,_/.li.J..ID.,.,e'--'c"'h-"'.s"--'f'--..,.C,'-"t,'-'-/a14.L.J.r1...,(...u\C.,___ ____________ _
2.) Client L.oca.tion; Slw/6!/ } ;Jc
3.) Date: __ 3C.<.J/c.....c1.w/9_,_$' __
1
4.) Well ID Number ~ -s, S.) Sampling Sequence#: __ __,,0'--~'----
6.) Sampler's Name: __ ....... ( 1-J.t<bo,...,_is _,_QLY.uf.w.lA[JJ,!w.,_____,_,,!kz""'·CL.C---413""'1-fwd=---
7.) Evacuation Method: --'""--Bailer
8.) Samplin:~ Method: ---'-'-Bailer
___ Airlift Pump
___ Bladder Pump
9.) Field Observations and Sampling Conditions
9.1) Outside Temperature: 7.. D C'C)
Weather Conditions: Clear _--1-_Cloudy
9.2) Was the well locked upon arrival? ___KYes
___ Bladder Pump
___ ID Number
___ Other
Calm __ Wmdy Ra.in
No
9.3) At.,y unusual conditions in the area? Yes -1.._No
If "Yes' explain:
I 10.) ·well Evat:uation (all measurements arc referenced from the top of tho well casing)
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10.l) Ca!;ing Diameter (ID): 2 . @ (mches)
10.2) Tc,tal Well Depth: 5 'I . 'iO (feet)
10.3) Stutic Water Level: '.2-? . / (., (feet)
10.4) Height of Wate: Column: 3 /,; .-...3.!L__ ~ (10.2 -10.3)
10.S) W11.ter Volume Ill Well: '2 7.. • ~ ~Gallons) ·
10.6) Evacuate ___J__. op Well Volumes Prior to Sampling
10.7) Ev.ocuate ---1a:is.._. 6D ~Gallons) Prior to Sampling (10.6 • 10.S)
Time Evacuation Started O'i : ~ S (Use 24 Hour Tune)
'lune Evacuation Completed ( 0 :~_"' so 24 Hour Tune)
10.8) Actual Volume Evacuated 'f J.. O)J _ ~allons)
10.9) Did the well go dty? Y, Yes ___ No /
A) Time well went dry _JQ_: / D Date 3 ~ 7 ~~
B)Timewellwassampkd/2. :QQ Date J. 7/ 5
C) Tot.al time between evacuation and sampling / hr i;o MIA (Hours)
I I.) Groundwat<,r Elevation
I I. I) Surveyed Well Elevation (MSL) ______ (feet) Data Not Available ___ _
I 1.2) Static Water Level Z.?, 1 //p (feet)
11.3) Static Water Elevation (MSL) ---------'-(feet)
d;\misc-frm\gmdwt.wp
10 029
12.) Well Sampling Dallt
12. I) Sample Collected
Test Parameters Bottlo Typo Size Preservativo Number Collected
7/ f)(, UreJI cf ci ,h1 ~ e l~·vSDu :J
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12.3) Sample Appearance: . X. Clear ___ Sediment Turbid
12.4) Samples placed on ice immediately after collection: L_ Yes ---No
13.) Field Analyses
Parameter
Temperature C'C)
pH
Conductivity
(uS/cm)
Types of pH Buffers Used:
I d:\mi,c-fnn\gmdwt.wp
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Calibration Std.
NIA
4.o /,.o .
I 15Z>O
4.0
7.0
Sample Reading
/9,~
7-6%
(07
Lot Number -------Lot Number -------
10.0 Lot Number -------
Std. After Sample
NIA
fri.Cf1
9<8A
10
2
030
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Well ID -~q"---)~q __
' -14.) Purge Summary
O3079~ 3(1 /q~ 3/ 7 /'15
Dale & Time -0'1'-/5 I-, Hfl
.
I h ,_,
Volume Purged L,t. 7-3 4/o ~~u A&
Well Temperature
lJ
ti.o /1.'f ,~,1 (·C)
Well pH Reading 5.~7 ~ .f'r, l,&i
Conductivity /0~ I ?73 (07 (uS/cm)
Other
Remarks vt~
1,\:1'
15.) Well secured with lock after =npling? _/_ Yes No
16.) I, the undersigi1ed, hereby certify that all of the above information is accurate.
Signature _("--'-'-=L-=-D~u~-ffi~& -
NOTE: Certain info!'mation (such as well elevations and mean sea level heights of well casings) cannot be
filled in on thls form unless provided to IEA personnel by the clienL
d:\mise-frm\gmdwt.wp
10
3
031
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1..tl-\.
NI AQuarion Company
I.) Client 1~ amc:
GROUNDWATER FIELD SAMPUNG DATA SHEET
!EA, INC.
/./1>cchsf le /a 11 t,<,t
2.) Client l.ocatim;: SJe/611 '1 I
;Jc
3.) Date: 3[1 /q~
I
4.) Well ID Number C,-~ 5.) Sampling Sequence #:
6.) Sampler':; Name: C.ba,s dui:la,;i ~ 811ad
•
7.) Evacuatio11 Method: ___ Bailer
8.) Sampling Method: ___ Bailer
---Airlift Pump
___ Bladder Pump
___ Bladder Pump
ID Number ---
9.) Field ObservatiollS and Sampling ConditiollS
9.1) Outside Temperature: ). ']....
td
Weather Co11<litio11S: Clear
("C)
=.i,_Cloudy
_j_ Yes
Yes
Calm
No
_.JL_NO
__ Wmdy
9.2) Wss th,:: well locked upon arrival?
9. 3) Any unusual conditiOllS in the area?
If •y,,..• explain:--------------------------
10.) ·Well Evacuation (all measu=ents are referenced from the top of the well casing)
10.1) Casing Diameter (ID): '.).. • OD (mches)
10.2) Total Well Depth: ___iQ___._QJ,2_ (feet)
10.3) Static Wat,;r Level:~ _ • .3.!:i_ (feet)
10.4) Height of Water Column: 3(p • .....Q{g__ (feet) (10.2 -10.3)
10.5) Water Volwnc in Well: 5 . '?le -(Liters/~ ·
10.6) Evacus.tc 3 -~Well-Vol~ Prior to Sampling
10.7) Evacuate /'l . .JL1L_(Uters/G~ Prior to Sampling (10.6 • 10.5)
Time, Evacuation Started {') : '2..0 .(Use 24 Hour Tune)
Tune Evaeuatlon Completed /?, 4 '5 (Use ~our Tune)
10.8) Actual Volume Evacuated /g . 'Cll) (liters/CZ~
10.9) Did the well go d.ty'! ___ Yes X No
A) Time well went dry ~J A-:____ Date
B) Tune well wss sampled / 3 : tJcS Date -3-,.../1-+/:-t-f~--
C) Total time between evacuation and sampling (Hours) -----------
1 I.) Groundwater Elevation
I I. 1) Surveyed Well Elevation (MSL),--______ (feet) Data Not Available_-:,:: __
11.2) Static Wat:r Level {? /N (feet)
11.3) Static Wat,.,r Elevation (MSL) _________ (feet)
d:\misc.fnn\gmdwt.wp
10
1
Rain
032
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Well ID (1~,_-_1._9_,___ __
12.) Well Sampling DaL,
I 2. I) Sample Collected
Test Parameters Bottle Typo Size Preservative Number Collected
-inc \.J1cJ 'tll..J 1-L~Di+ 7.
"6:z. lf-D vcJ! I/OJ He( 3
12.3) Sample Appearance: y Clear ----,-Sediment Turbid ---
12.4) Samples placed on iee immediately after eolleetion: -X-Yes No
13.) Field Analyses
Parameter
Temperature (°C)
pH
Conductivity
(uS/cm)
Types of pH Buffers Used:
d:\misc-fnn\gmdwt.wp
.
Calibration Std.
NIA
4.C> f,.D .
I rs757,
4.0
7.0
· Sample Reading
,~.r
~( 31
--z._ y.,
Lot Number -------LotNumber -------
10.0 Lot Number -------
Std. After Sample
NIA
w.C/~' ..
qrr
10
2
033
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Well ID C -4'3 3
14.) Purge Summ.uy
3/1 /Ci<; -ft1 ( Dale & Time
,";7ri
Volume Purged ]Jlt. l_p 11-I~ Q(\~ ~rt,•
Well Temperature
d D
(°C) 11.tj /1-3 (1,7 (& c; lt, ~
Well pH Reading 5:i7 5 6 ,, ' o( S.>O ~,) \ '5,27
Condu.:tivity S3 J_~ 27 2i/ :z. 3 (uS/cm)
Oth,,r
Remarks
15.) Well sccutcd with lock after sampling? __J,_ Yes No
16.) I, the under:signed, he<cby certify that all of the above information is accurate.
Signature_~ ·-+c-+-~-·. ~Oc~~-6P::-Date_____,j~· /1j....!...;;_/1s __
NOTE: Certain. information (such as well elevations and mean sea level height.. of well casings) cannot be
filled in on this form unless provided to IEA per:sonnel by the clienL
d:\misc-frm\gmdwt.wp
lQ 034
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M Aqua,ion Company
GROUNDWATER FIELD SAMPLING DATA SHEET
!EA, INC.
I.) Client Name: _...,.J/i~D~C~C~-h~.s~f~~Lt~t.~/a~fl~!~S-1: ____________ _
2.) Client l.ocation~ She/611 J NC
3.) Date: _ _..3,--17-'--+/_,_q (..___
7
I I
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4.) Well ID Number [f-~ 2-5.) Sampling Sequence#:---:-,__,_ __
6.) Sampler'., Name: __ _,.(,..,h ...... R ..... is_,O ..... d><-L-U..la ..... 1;)...__ __ ,,.-:--_/ i.lW';-~__,fh......_.,.~'-i'-="---'-----
1 .) Evacuation Method: ___ Bailer ___ Airlift Pump ___ Bladder Pump --~Other
8.) Sampling Method: ___ Bailer ___ Bladder Pump ID Number ---
9.) Field Obs,,rvations and Sampling Conditions
9.1) Outside Temperature: __ __,]..c..7,,--'--__ (."C)
Weather Conditions: Clear _1::,_ Cloudy
9.2) Was the well locked upon arrival?
9 .3) Any unusual conditions in the area?
___:,t_ Yes
Yes
Calm
No
--4-No
__ W'mdy
If 'Yes" explain:~-----------------------
10.) ·Well Evacuation (all measurements are referenced from the top of tho well casing)
10.1) Casini~ Diameter (ID): '.2--. oP (mches)
10.2) Total Well Depth: ft 1-~(foet)
10.3) Static Water Level: / J . (feet)
10.4) Height of Water Columii: • if:b (feet)(l~ 10.3)
10.5) Wawr Volume in Well: 7 . ). "l-(Liters/G~
10.6) Evacuate 3 . t1t> Well Volumes Prior to Sampling
10. 7) Evacuate '2-2-. u-0 (Liters/G~ Prior to Sampling (10.6 * 10.5)
· Time Evacuation Started {1 :]S__ (Use 24 Hour Time)
. TIIDe Evacuation Completed I', : Z. S' (Use 24 Hour Time)
10.S) Actual Volume Evacuated Zl . Ol) (Liters/~
10.9) Did the, well go dry? __ _,,,Yes )( No
A) T1IDe well went dry ;JI+: Date
B) Time well was sampled I(=--. :-1,-c; Date 2·'"'/'7--t-fq-:-rc:-----
,
C) Total time between evacuation and sampling ___________ (Hours)
I I.) Groundwater Elevation
11.1) Surveyed Well Elevation (MSL) _______ (feet) Data Not Available
1 l.2) Static W:iter Level /7.91' (feet) ----
1 l.3) Static Water Elevation (MSL) ___ -_____ (feet)
d:\mi1c-frm\gmdwt.wp
10 •
Rain
035
12.) Well Sampling Data
12.1) S.tmplc Collected
Test Parameters Bottle Typo
-1nC \} If
v7_t.//) \/1f,
Size
~o~
~o ,.,,J
Preservative Number Collected
R,~o~ t-
rk! s
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12.3) Sample Appearance: ~ aear ___ ScdimeD.t Turbid ---
12.4) Samples placed on ice immediately a&:-collection: __i_ Yes No
13.) Field Analy,;cs
Parameter
Temperature (°C)
pH
Conductivity
(uS/cm)
Types of pH Buffers Used:
I
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Calibration Std.
NIA
4,C> /-, ,D
'
I 1'i757">
4.0
7.0
10.0
· Saniple Reading
II, ,U
ln,1/f
7'i
Lot Number ______ _
Lot Number -------
Lot Number -------
Std. After Sample
NIA
In .99
c,<fl
10
2
036
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Well ID _ __,_p_f-_·~~~'}_-
14.) Purge Summary
Date & Time 3/1/0)
1 '-11 S
Volume Purged ]J,lt. ' IY
Well Temperature
(·C) !In.~ I~' I I&, i
Well pH R,,ading
~I 1i, 1.~1 lD, -s<o
Conductivity ~~ 1( 1g (uS/cm)
Other
Remarks
15.) Well secured with lock after sampling? ..A.... Y""
3
3/l~S" . .
l"l. <:;
7, i-(J.!tv.
u
!b, 0 /L,h
(o, 4g tp,c./.7
13 11
No
I 16.) I, the undersigned, hereby certify that all of the above information is accurate.
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Signature ---->,-C-,'1-l--'-'-""t-9-=--0,..._,loA-'-'JM ....... a=b-_
NOTE: Certain information (such as well elevations and mean sea level heights of well casings) cannot bo
filled in on this form unless provided to IEA personnel by the elienL
d:\misc•frm\gmdwt.wp
10 037
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lbl\
An AQuo,ion Company
GROUNDWATER FIELD SAMPLING DATA SHEET
!EA, INC.
1.) Client Name: _ .... //i ..... n=e__.c..,,h-"':.s"-'f~~0'-"t'-'-lo ......... 11.,.,f.~~t~-------------
2.) Client Location: SJe/0; I NC
1
3.) Date: 3 /7 l9. S--
4.) Well ID Number f ('-31 5.) Sampling Sequene<> fl: _ _._1-=c& ___ _
6.) Sampler's Name: ----l,,,C;.1,J,h-qis..i.....,,,,<d'-'<..dL..Ultr"-"w.,_____---__,_
,
,
/
w
,
=
'
-
~
b
=
V
f
1
d
-
J
"
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-
-
-
7.) Evacuati.on Method: ___ Bailer ---Airlift Pump
___ Bladder Pump
___ Bladder Pump
ID Number
.Other --~
8.) Sampling Method: ___ Bailer ---
9.) Field Observations and Sampling Conditions
9.1) Outside Temperature: 2! C'C)
W,:ather Conditions: Clear _JS...Cloudy Calm __ Windy Rain
9.2) Was the well loclced upon arrival? ___:;,t_ Yes No
9.3) Any unusual conditions in the area? . Yes _Js._No
If "Yes' CJCplain:
10.) ·well Evacuation (all mca.surcmcnts arc referenced from the top of tho well ca.sing)
10.1) Casing Diameter (ID): "2-• OP (inches)
10. 2) To'.al Well Depth! ;, q . 5 D (feet)
10.3) Sis.tic WatcE Level: i;, . 'ii 7 (feet)
10.4) Height of Water Column: '2. 0 . (g;, (feet) (10.2 -10.3)
10.5) Water Volume in Well: :?, • 3( (lltcrs/~ -
10.6) Evacuate 3 . ca;> Well Y~ Prior to Simpling
10.7) Evacuate ID • QQ {li!crf~ Prior to Sampling (10.6 "' 10.5)
1:'ime Evacuation Started __rt_: 'l. 0 (Use 24 Hour 'fime)
1~rme Evacuation Completed /4 S"O (Use 24 Hour Time}
10.8) Actual Volume Evacuated IQ • c,p (llters/~
10.9) Did the well go dry? ___ Yes ~~-No
A) Time well went dry 1/f :___ Date
B) T'tme well was sampled ( '( -

:

S:: 0 Date -3'/""1],.,/ -c-'i'S: __ _ . ;
C) Tc,t.al time between evacuation and sampling ___________ (Hours)
1 I.) Groundwate,· Elevation
11.1) Surv<>yed Well Elevation (MSL) _______ (feet) Oats. Not Available ___ _
11.2) Static Water Level /), 'l] (feet)
11.3) Static Water Elevation (MSL) ___ -_____ (feet)
d:\m.i5e-frm\gmdwt.wp
10 038
Well ID 2
12.) Well Sa.mpliog Daill
12. I) Sample Collected
Test Parameters Bottle Typo Size Prescrvativo Number Collected
10G 1)1cJ. UOvM +L \bl£ 1
<;,7,. t.{t) 1110. u Yo ... f.lU '½
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I 12.3) Sample Appearance: ,k, Clear __ &diment Turbid ---
12.4) Samples placed on iee immodiatcly after collection:_)(_ Yes No
I 13.) Field Analysc:s
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Parametei:
Temperature ("C)
pH
Conductivity
(uSlcm)
Types of pH Buffers Used:
I d:\mise-frm\gmdwt.wp
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Calibration Std.
NIA
. 4.C> /,,◊ .
/C5DT)
4.0
7.0
10.0
Sample Reading
/0_,1)
Y.10
I ti3
Lot Number-~-----
Lot Number ______ _
Lot Number -------
Std. After Sample .
NIA
(n,c;q
qq9
10 039
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Well ID _FL....JrL---....:,3=-----4,__ 3
14.) Purge ~:umrruuy
Date&. Time ?:>/i /c;c; 3/1/fs
1410 i4SD
Volume Purged ]JJt. 3 ~ IDIM.I 1 'ffA
Well Temperature
V
I~,{ (•q \~.1-/In, D /1,,1. 16.o
Well pH Reading ~.~~ ~,If 0 ' /., i./ 9,7D 9,7;..
Conductivity 10 13 90 !OS (uS/cm) 102-
Other
Remarks
15.) Well secured. with lock after sampling? _L_ Yes No
16.) I, the undersigned, hereby certify that all of the above information is accurate.
Signature _ _;,....,C:J,..l.i.l.i.:kv-1:,:___ . ..i.;,.LJ,LJJfo=¼v -. Date ----"'3'-l-'!-/1,-i-l-/qc-;.,__· __
I I
NOTE: Certain information (such as well elevations and mean sea level heights of well casings) cannot bo
filled in on this form unless provided to IEA personnel by the clicnL
d:\mise-frm\gmdv.1..wp
10 040
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M AQu.:,rion Company
1.) Client Name:
2.) Client Location:
3.) Date:
4.) Well ID Number
6.) Sampler's Name:
GROUNDWATER FIELD SAMPLING DATA SHEET
!EA, INC.
i-/Dechsf Ce/4ot{t
01:1'' ;Jc
FP~2-'3 5.)
C.bRis Ovl:la,;}
Samp~ Sequence //:
>fk t;M(Mi
l
13
7.) Evacuation Method: ___ Bail.er ___ Airlift Pump ___ Bladder Pump )( . Other
8.) Samplin1; Method: ___ Bailer ___ Bladder Pump ID Number ---
9.) Field Observations and Sampling Conditions
9.1) Otr.tsidc Tcmpe:atnre: ZI (."q
W,:ather Conditions: Clear _X_Cloudy Calm __ Windy Rain
9.2) W•s the well loclced upon arrival? _LYCS No
9.3) ~y unusual conditions in the area? Yes _'f.._No
If 'Yes• explain:
10.) ·well Evacuation (all measurements are referenced from the top of tho well casing)
10.1) Casing Diameter (ID): 'l . /JD (rnchcs)
10.2) Total Well Depth: 2.:, . I.ab (feet)
10.3) Static Water Level: I 2, • ;de Ii, feet)
10.4) Height of Water Column: / 0 . "l. (feet) (~O -10.3)
10.5) Water Volume in Well: _ _,___. (Liters/G cins .
10.6) Eva,::uato ±· @ Well Volumes Prior to ling
10. 7) EvBJ:uatc · • t7l) (Liters/G~rior to Sampling (10.6 * 10.5)
'lime Evacuation Started I ~ uL (Use 24 Hour Time)
Time Evacuation Completed / S:: : or (Use 24 Hour 'Iµne)
10.8) Actual Volume Bvac:uated S:: . 6l) (Liters/@o~ .
10.9) Did llho well go dzy? ---,-,crYes _c...__No
A) Time well went dry ,\M. :___ Dato_.,......, ___ _
B) T11ne well WU sampled ( f. : D '> Date -~'.:2..,/i--J't-/ £~~'--
q Toi:al time between evacuation and sampling ___________ (Hours)
11.) Groundwater Elevation
11.1) Surveyed Well Elevation (MSL) _______ (feet) Data Not Available ___ _
11.2) Static Water Level /';\, 3(, (feet)
11.3) Static Water Elevation (MSL) ___ -_____ (feet)
d:\misc-frm\gmdwt.wp
10 041
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Well lD -~t.._t~-7,_c.......:7).,__
12.) Well Sampling Data
12.1) S"mple Collected
Test Param,oters Bottle Typo
'JDC Vt"o. U
Size
~OIYVJ
Preservative Number Collected
µ,(rx, 7_
'
'
12.3) Sample Appearnnce: . :6, Clear ___ Sediment ___ Turbid
12.4) Samples placed on ice immediately after collection: _J.._ Yes No
13.) Field Analyses
Parametiir
Temperature ("C)
pH
Conductivity
(uS/cm)
Types of pH Buffers Used:
d:\mis.c-frm\gmdwt. wp
Calibration Std.
NIA
4.C> {-, . D .
/125r)
4.0
7.0
10.0
Sample Reading
Lot Number ______ _
Lot Number -------Lot Number -------
Std. After Sample
NIA
(,. _q9
m
·10
2
042
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Well ID _ __._r..!.-r_✓_:_i_-,_ 3
14.) Purge Summary
Date & Time 3Til'l5' 3hh~
)45'5" /505
Volume .Purged JJJ+. I. S' ? 'I) ;-.oqJ AffJA
L
Well Temperature IS.~ \S,1 li,x-1<;, 5 /5, (p (·C)
Well pH Reading 1,2-) Co,31 fo,07 /p, I I G,09
Conductivity 6 ;;_ 50 S-L/ ~2. 54 (uS/cm)
Other
Remarks
15.) Well secured with lock after sampling? _L Yea No
16.) I, the undersi1;ned, hereby certify that all of the above information is a=rato.
Signature---'-"'C~~a~~="-a,.___,-Dato __ 34-/...,__,1/,_,_1..::_.> __ _
NOTE: Certain information (such as well elevations and mean sea level heights of well casings) cannot bo
filled in on this form unless provided to IEA personnel by the client.
d:\misc•frm\gmdwt.wp
10 043
,i !E.i~y
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GROUNDWATER FIELD SAMPLING DATA SHEET
!EA. INC.
I.) Client I-lame: _ _,_//i..uD.,_,(o-.1C..,_,_h-".s"'-f'----"Lt ... e'-'-la...,..11 .... f.w<:. t~-------------
2.) Client Location: __ ..,.S ..... AweCLli ... i:,..Ll_,,--..<-Mcc..:C,:c_ _____________ _
3.) Date: _ __._3'+"'/~+-'/c1~f_--/
4.) Well ID Number _~E=J;_-~f_'6 __ --::c---5.) aling Sequence II: ;!I
6.) Sampler's Name: ___ C, ...... ba ...... is~O~d.,_._la ........ w..__ __ lA=m~-6=Mf-ad=~--
7.) EvacuatiC1n Method: ___ Bailer
8.) Sampling Method: ___ Bailer
__ Airlift Pump
___ Bladder Pump
___ Bladder Pump
___ ID Number
9.) Field Obsorvations and Sampling Conditions
9.1)
9.2)
9.3)
Outside Temperature: --~J~D __ ~C)
Weather Conditions: Clear __y Cloudy
Wa,: the well locked upon arrival?
Any unusual conditions in the a=?
___:;t_ Yes
Yes
Calm
No
_J_No
__ W-mdy
If 'Yes" explain: --,-----------------------,--
10.) · Well Evacuation (all mea.surcmcnts are ref=nccd from the top of tho well ca.sing)
10.1) CasiI1g Diameter (ID): 1-. . OD (mches) . .
10.2) Total Well Depth! 5 i5 • oV (feet) .
10.3) Staib Wal.er Level: 4D~d3)
10.4) Height of Water Column: ~ (feet) (10.2 -10.3)
10.5) Wsu.r Volume in Well: ,i . (liters/~ ·
10.6) Evac:iiate ___J__. (8) Well -Volumes Prior to Sampling
10.7) Evac11atc ~-@ (Iltus/~Prlor to Sampling (10.6 • 10.5)
Tbne Evacuation Started ~-(Use 24 Hour 1ime)
Tune Evacuation Completed . : I (Use 24 Hour 1ime)
10.8) Actual Volume Evacuated ---'--· () (Il~
10.9) Did tho well go dry? ---,r, Yes J No
A) TIIllle well went dry N~---
B) Tun• well was sampled --~-'--'-: . ...,\.,,C)<--_
Date .,.-,--=-,,-,,---
Date Q:?, Q2, "lS
C) Total time between evacuation and sampling ___________ (Hours)
11.) Groundwater Elevation
1 I. 1) Survey-od Well Elevation (MSL) ______ (feet) Data Not Available_-::_-:: __
I 1.2) Static Water Level t./0, /7 (feet)
11.3) Static Water Elevation (MSL) ___ -_____ (fect)
d:\misc-frm\gmdwt.wp
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Rain
044
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12.) Well Sampling Data
12.1) Sample Collected
Test Parameters Bottle 1)'po
'/OC l/1a. ()
~1-J-/O v1r,
Siz.e
4liAM
6
1/(1,r,J
Preservative Number Collected
JI, S 0'! 2-
• 3 JIU
'
12.3) Sample Appearance: _j__ CJ.ear ___ Sediment Turbid ---
12.4) Samples placed on ice immediately after collection: _i__ Y cs No
13.) Field Analyses
Parameter
Temperatun, (°C)
pH
Conductivity
(uS/cm)
Typos of pH Buffers Used:
d:\mise-frm\gmdwt.wp
Calibration Std.
N/A
4.C> (7.0
'
ll5l5n
4.0
7.0
10.0
· Sample Reading
It I
Lih
¥1
Lot Number -------Lot Number -------Lot Number -------
Std. After Sample
NIA
L,q1
((%0
10
2
045
I Well ID _____f.~ -s~
I I
· ·· 14.) Purge Summary
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3/~ 9~ Date & Time
()c ttJ(
Volume Purged L-,Jt. ) ~
Well Temp,:raturc ,q,O (g;t ,~,i (·C)
Well pH Rc:ading t.1~ t. 81 6. is
Conductivity ( )_)._ ~2$' '33 (uS/cm)
Other
Remarks
15.) Well secured with lock after sampling? __)__ Y cs
31r(c;s'
rf), It, -
qqJ A raj\
I
rt/ I 'ff,3
6.9b {13
~7 87
No
I 16.) I. the undersigned, b.crcby certify that all of the above information is accurate.
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Date 0>~'17
NOTE: Certain information (such as well elevations and mean sea level heights of well casings) cannot bo
filled in c,n this form unless provided to IEA personnel by the clienL
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3
II 10. 046
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M "-Quarion Company
I.) Client Name:
2.) Client Location:
3.) Date:
GROUNDWATER FIELD SAMPLING DATA SHEET
!EA, INC.
tfoe,h5f Ct.la11t£t
SAe/611 ,· Ale
l
3k(qs r1
4.) Well ID Number -i-;i 5.)
C.hizis Ovtlew
Sampling Sequence /I: ~--!-( ___ _
q;im 641od:
6.) Sampler':; Name:
7,) Evacuation Method: ___ Bailer
8.) Sampling Mcthod: ___ Bailer
---Airlift Pump
___ Bladder Pump
___ Bladder Pump
___ ID Number
I Other
I 9.) Field ObS<:rvations and Sampling Conditions
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9.1)
9.2)
9.3)
Outside Temperature: --~2~D~ __ ('C)
Weather Conditions: Clear __,l_ Cloudy
Was the well locked upon arrival?
Any unusual conditions in the area?
_lS-Ycs
Yes
C.alm
__ No
__3'.._No
__ Windy
If •y cs• explain: --:----------------------,--
10.) ·well Evaeuilion (all measurements are referenced from the top of the well casing)
10.1)
10.2)
10.3)
10.4)
10.5)
10.6)
10.7)
Casing Diameter (ID): 2 . QO (mchcs)
Total Well Depth: -2L-~ (feet)
Stati,: Water Level: __J_!j_ . ...J.!i__ (feet)
Heigb.t of Water Column: Y "'J. 7 ~ (feet) (l<y..=..,10.3)
Water Volume in Well: '7 . II (Uters/G~ ·
Eva.ciiate :~ • cq, Well .Y~Prior to Sampling
Evacuate -rr. t70 (Liters/ allons Prior to Sampling (10.6 '" 10.5)
Thne Evacuation Started Q q : (Use 24 Hour 'Thne)
Tune Evacuation Completed /1) : 1. S" (Uao ~our 'Thne)
10.8) Actual Volume Evacuated 1:1-: m) (Uters/G~
10.9) Did the well go dr:y'I --,-r-r Y cs IX No
A) Tune well went dry Vif =~--Date-.,,.,,,,~-,,---
B) Tim,, well was sampled IV. : 1't Date __ 34/9~/ .... · q..,{ __
C) Total time between evacuation and sampling ________ t ___ (Hours)
11.) Groundwater Elevation
Data Not Available
Rain
I I. l)
l l.2)
I 1.3)
Survey,od Well Elevation (MSL) ______ (feet)
Static Water Level _ _._lg~ .... 7 ... '{ ___ (feet)
----
Static Water Elevation (MSL) ___ -_____ (feet)
d:\misc-fnn\gmdwt.wp
10 047
12.) Well Sampling Dall\
12.1) Sample Collected
Test Parametera Bottle Typo
'Toe ,J,cJ
..
Size Preservative Number Collected
<./0 rJ /{ \Ov 8-.
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12.3) Sample Appearance: ?( Oear ___ Sediment ___ Turbid
12.4) Samples placed on ice itnmcdiately aftet collection: _L_ Yes No
13.) Field Analyses
Parameter
Temperature (°C)
pH
Conductivity
(uS/cm)
Types of pH Buffera Used:
I dclmi«-fnnlgmdwt.wp
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Calibration Std.
NIA
1-/-.C> /-, -D
•
/ 1575r)
4.0
7.0
10.0
Sample Reading
10,~
In, Q(;
c;°t~
Lot Number ______ _
Lot Number -------Lot Number -------
Std. After Sample
NIA
&,11·
I lJvV
10
2
048
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I ; ___ 14.) Purge Summary
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Date & Time 3/Slq( -3~(q(
t)qi.( < 16,~
Volume Purged vi+. 7 }4 z2aJ
Well Temperature )0,0 ~
(°C) ,~' ~ 1~.o /1 '~
Well pH R,:ading 5, tb 5,q) 6. ;I l. Ob
Conductivity ~11 5io s~:2, s19 (uS/cm)
Other
Remark,
15.) Well secured with lock after sampling? _L Yes No
.
Nlet
11,,
w,oy
---
s-15"
I 16.) I, the undenigned, hereby certify that all of the above information is accurate.
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Signature-----1-L~~_.,._,.QJ]i--"-"-"--_
NOTE: Certain iinformation (such as well elevations and mean sea level heights of well casings) cannot bo
filled in on this form unless provided to IBA persoonel by the clienL
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Ari AQua<ion Company
GROUNDWATER FIELD SAMPLING DATA SHEET
!EA, INC.
!.) Clienl Name: _ ..... Yi~t,=e~c.=h~..s~f~~Li~e~la~a~r.~~t _____________ _
2.) Client Location: --~&~b.,..R~b~~-=t-l(--JJ>-'-N{~C,~--------------
,3/r lc 5 7
3.) Date: -----=--+.--"1+-t"--'~-
I
4.) Well ID Number __ --1-l_-_3.cc-c;_____ 5.) Scg Sequence /1: -~!~(, __ _
6.) Sampler's Name: __ • _.(.,...h._.,_.a._...is._d"-L."-vl:UJlau..>1;).,___....,_/4rn"'--'-!-!. --'--"'/1 ...... w,...,l..,.,.,l'Ul=d:..___ __
7.) Evacuation Method: ___ Bailer ---Airlift Pump ___ Bladder Pump
8.) Samplint: Method: ___ Bailer ___ Bladder Pump ID Number
9.) Field Observations and Sampling Conditions
9.1)
9.2)
9.3)
Outside Temperature: 1 0
W.:ather Conditions: Clear
Was the well locked upon arrival?
Any unusual conditions in the =7
('C)
~ Cloudy
_J-Yes
Yes
---
Calm
No
--1LN0
__ Windy
If 'Yes" explain: --------:--------------------,---
10.) ·well Eva,:uation (all measu=ents arc referenced from the top of tho well casing)
10.1) Ca,:ing Diameter (ID): / • ~ (inches)
10.2) Tc.ta! Well Depth: 3 S: .--1.D..,_ (feet)
· 103) Stutic Wa1t:,r Level: /<I; _ • ...i5:,_ (feet)
10.4) Hdght of Water Column: '.).. I • / $ (feet) g!J4 -10.3)
10.S) Water Volume in Well: ? . Y'{ (Liters/~) -

-
10.6) EvacW!te 3 -~ Well V~;~ Prior to Sampling
10.7) Evacuate I I .___{JQ_(Llters/ allo Prior to Sampling (10.6 * 10.5)
Time Evacuation Started O'i' : D (Uso 24 Hour Time)
Time Evacuation Completed ID _:-3.1)___ (Use ~our Time)
10.8) Acwal Volume Evacuated f / -~0'1/-"--(I.i (Uteters/G~
10.9) Did tho well go dty7 ___ Yes -~-No
A) Time well went dry A/ : Date , 1
B) 1ime well was sampled r I◊--,---t,o Date _-::_-::_-;:/:&';_f-/q':_s'.:,-::_-::_-
C) Total time betweeu evacuation and sampling ________ , -'-___ (Hours)
11.) Groundwat,,r Elevation
11. I)
11.2)
11.3)
Sur'leycd Well Elevation (M~L) _.,.,_ ______ (feet)
Static Water Level /'i -S'S (feet)
Static Water Elevation (MSL) ___ -_____ (feet)
d:\mi$c•frm\gmdwt.wp
Data Not Available ----
10
Rain
050
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12.) Well Sampling Data
12. l) Sample Collected
Test Pa.ra.metera Bottle Typo Si.zc Preservative Number Collected
,,-()G (/1e,,., 1dJ H. (nu 1
67-~ V 1/(Cu ~vJ #(/ 3
..
12.3) Sample Appearance: ✓ Oear ___ Sediment Toroid ---
12.4) Samples placed on ice immediately after collection: _L._ Yes No
13.) Field AnalyS<:s
l'arametel~
Temperature (°C)
pH
Conductivi~,
(uS/cm)
Types of pH Buffera Used:
d:\misc-frm\gmdwt.wp
Calibration Std.
NIA
4.c /,.o .
1rv,r-,
4.0
7.0
10.0
Sample Reading
20,3
1.,0
{JO
Lot Number -------Lot Number -------Lot Number -------
Std. After Sample
NIA
& ,q,
,auo
10 051
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r.l ->r Well ID _ ___, __ .><-2..::::) __
14.) Purge Summary
Date&. Time ~t:
Volume Purged LN+.
Well Temperature !1 .I (°C)
Well pH Reading 5,56
Conductivity £37 (uS/cm)
Other
Remark,:
3
-31f;hr
lo 1io
q ~ {I cuJ I f~A
1tO ).O, I r Jo. "Y r ~
5,71 5,5 3 5.5a 5,5~
619 6./5 &30 . lll
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··. \ 15.) Well =red with lock after sampling? _L_ Yes No
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16.) I, the undersi1~, hereby certify that all of the above information is accurate.
Date __ 3+19-+/_q_j __ _
NOTE: Certain information (such as well elevations and mean sea level heights of well casings) cannot be
filled in on. this form unless provided to IEA personnel by the client.
d:\misc-frm\gmdwt.wp
10 052
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.l. L J. .>..
An AQua1ioo Gompany
GROUNDWATER FIELD SAMPLING DATA SHEET
!EA, INC.
-1 -/7 17
4.) Well ID Number----'------'----.,,..---5.) S~g Sequence II:
6.) Sampler's Name: __ _.(.,,,...hµ,Q ..... is.__O""'-'<..vtUJIA'-'-"WU--....:~~-'-""fli-t1.,.,..1-=Mi'--"-'----
1
7.) Evacuati.on Method: -~X~Bailer ___ Airlift Pump ___ Bladder Pump Other --~
8.) Samplin1; Method: -~(_Bailer ___ Bladder Pump ID Number ---
I 9.) Field Observations and Sampling Conditions
I
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9.1)
9.2)
9.3)
01,tside Temperature: 10
W,:ather Conditions: Clear
W,s the well locked upon arrival?
Any unusual oonditioas in the area?
If •y cs. explain:
(."C)
_1,___Cloudy Calm __ Wmdy
_£__Yes No
Yes _,&_No
I 10.) · Well Evacuation (all measu,cments arc referenced from the top of the well casing)
10.1)
10.2)
10.3)
10.4)
10.5)
10.6)
10.7)
Casing Diameter (ID): ,J . qp ('mchcs)
Total Well Depth! __/__l__._.5j___ (feet)
Static Waf.cl: Lev~~ . 4 I (feet)
Height of Water Column: o/ . 0 ~ (feet) (10.2 -10.3)
Water Volume in Well:-~-· .gzr--0:iQGallons)
Evat:itate ,3 • qt> '?{-cll;Vo~Pn-;; to Sampling
Evru::uate /J • 01.) ~G o Prior to Sampling (10.6 • 10.S)
Time Evacuation Started Oq : ~ (Use 24 Hour Ume)
11'me Evacuation Completed 09 : 9 O_jpao 24 Hour Thne)
10.8) Aetu.tl Volume Evacuated 4 . 00 <L½#Gallons)
10.9) Did the well go·dty'l __ ~Ycs X No
A) Time well went dry i\)~ : Date
-
B) Time well was sampled' Qq ~ -. :-Lj~(J Date _:_-:::.1::!:x:./1~(~-=--=--
C) Total time between evacuation and sampling ___________ (Hours)
I I.) Groundwater Elevation
Raia
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I I. 1) Surveyed Well Elevation (MSL) .-------(feet) Data Not Available ___ _
I 1.2) Static Water Level /'5. YI (feet)
I 1.3) Static Water Elevation (MSL) -(feet) --------
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10 053
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12.) Well Sampling Data
12.1) Sample Collected
Test Parameters Bottlo Typo
"!tiG v,J
Size
¼Q,.,.J
Prcservativo Number Collected
JI. (ou .:J
'
12.3) Sample Appearance: ___ Clear ___ Scdime.nt ,/ Turbid
12.4) Sampl::s placed on ice immodiately after collection: ---4--Yes No
13.) Field Analyse,:
Parameter
Temperature (°C)
pH
Conductivity
(uS/cm)
Types of pH Buffors Used:
d:\misc-fnn\gmdwt.wp
Calibration Std.
NIA.
4.t> {-,.()
•
ICioD
4.0
7.0
10.0
Sample Reading
1i.s
5. Y1
5Y(
Lot Number ______ _
Lot Number ______ _
Lot Number · -------
Std. After Sample
NIA
(o ,~1
' lfffll
10
2
054
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Well ID __ .,,,--.,__/_·..,_/--'-7 __
I
• ·-14.) Purge Summary
Dale & Time 3/iq{
09 0
Volume Purged LJt.
Well Temperature /?,C) (·C)
Well pH R,:ading 5,~g
Conductivity 598 (uS/cm)
Other
Remarks
'/ 3
/17 /'1, 3
~qq S,Y~
S6 I 5S6
15.) Well secured with lock after sampling? ___L.. Yes
3
3/gl"I>
09£/0
t./-);1 !l{kfl-
/3,5 /?,, ~
5,31 ),)7
54(; 54]
No
I 16.) I, the undersigiacd, hereby certify tha\ all of the above information is accurate.
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Signature~(-'--=-~-O_JJ w-__
NOTE: Certain information (such as well elevations and mean sea level heights of well casings) cannot bo ; ·
filled in on this form unless provided to IEA personnel by the client. '
d:\mise--frm\gmdwt.wp
10, 055
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lbl-\
Ari Aqu.irion Company
GROUNDWATER FIELD SAMPLING DATA SHEET
!EA, INC.
l
I.) Client Name: --'-lli..lJ{).,_,,e...,,.,_,_.h..,:,5::,_f,_...,.lt'""t:"-la>U.!r1-"'(.u.J\e"'-----
-
-
-
-
-
-
-
-
-
-
-
2.) Client Location: SAe/6:f J NC
3.) Date: _ _..i.3.L..J../!LJ...r/0-'-") __
I I
4.) Well ID Number Ii.Ii. -~¥_ 5.) Sampling Sequence /I:
6.) Sampler's Name: ChRis dtrtla,~ 2k &t4cnf
7.) Evacuation Method: Bailer Airlift Pump Bladder Pump
8.) Sampling: Method: Bailer Bladder Pump ID Number
9.) Field Ob,:ervations and Sampling Conditions
9.1) Outside Temperature: io C'C)
Weather Conditions: Clear _L_Cloudy Calm __ Windy
9.2) Wa, the well locked upon arrival? _[._Yes No
9.3) Any unusual conditions in the area? Yes _L_No
If "Yes" explain:
10.) ·well Evacuation (all measurements arc referenced from the top of the well easing)
10.1) Casing Diameter (ID~:. . Oi) (inches) .
10.2) Total Well Depth: • llD (feet)
10.3) Static Waler Level: L~ (feet)
10.4) Height of Waler Column: ~_.3.L (feet) (10.2 -10.3)
10.5) Water Volume in Well: _ __,__,.....s:.L (Liters!G@)
10.6) Evacuate 3 . p];> Well Volumes Prior to Sampling
10. 7) Evacuate 5 . CJ/) (liters/~) Prior to Sampling (10.6 " 10.5)
Tune Evacuation Started / I : O'> (Use 24 Hour Time)
Tune EV11CW1tion Completed r I I : l:{,,D (Uso 24 Hour Timo)
10.8) Actual Volume Evacuated S: . Q1l (Litersl@s)
10.9) Did the well go dry? --~ Yes X No
A) Ttme well went dry A/.A :.___ Date ~,,i'~---
B) 'lim,, well was sampled /I : !!,o Date :;/ l?/ 95
R
( I
C) Total time between evacuation and sampling ____________ (Hours)
11.) Groundwater Elevation
. Other
Rain
1 I. 1) Survey,:d Well Elevatioo (MSL) _______ (feet) Data Not Available ___ _
11.2) Static Water Level ~ ¥'., (d (feet)
11.3) Static Water Elevation (MSL) ___ _. _____ (feet)
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10 056
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Well ID
12.) Well Sampling Da~,
12. I) Sample Collected
Tc>t Parameters Bottle Typo Si:rc Pre.servativo Number Collected
'JOG v1c.J ~o..J ff, SD-.f J
<;;q,.. ~ /) v,J ~v..,J /IC/ ;,
12.3) Sample Appearance: . )( Clear ___ Sediment Toroid ---
12.4) Samples placed on ice immcdiatcl.y after collection: ___;f,_ Yes No
13.) Field Analys,,s
Parameter
Temperature ("C)
pH
Conductivity
(uS/cm)
Types of pH Buffers Used:
d;\mise-frm\gmdwt.wp
Calibration Std.
NIA
4.6 f-,.D .
l152>D
4.0
7.0
10.0
· Sample Reading
Jq Si
~.1'S
s~
Lot Number -------Lot Number -------Lot Number -------
Std. After Sample
NIA
G ,q,
!lf'u'D
10
2
057
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Well ID
14_) Purge Summa,y
~~/9< 3~~ J
Date & Time -q(
11~< 'o
.
Volume Purged L,it. I, 5 3,D q.o~J ~lff;,
Well Temperature
C>-J l/1 ,9 ,~. i (0,5 ;?, ? l~,3
(°C)
Well pH Reading &,~/ /o/2,/ {OJ 5,tS 51 io
Co11ductivity lo~ 06 {() 51 59
(uS/cm)
Other
Remark,;
lS.) Well secured with lock aft« sampling? _L Yes No
16.) I, the undersigned, hereby certify that all of the above information is accurate.
Signature----'"'C~L-+,<-U---"----"-=~~
NOTE: Certain information (such as well elevations and mean sea level heights of well casings) cannot be
filled in 011 this form unless provided to IEA person11el by the client.
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3
10 058
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J_ .L.J .L ,...
An Aqu<lfion Company
1.) Client Name:
2.) Client Loeatio11:
3.) Date:
GROUNDWATER FIELD SAMPUNG DATA SHEET
!EA. INC.
!-loecn.51 Celan(St
SAR/611}
3)1 ttt { -r
Ale
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4.) Well ID Number G G -~/ 5.)
(.hais dvi:la,;i
Seling Sequence fl: _ __c/_'1 ___ _
tM 6u1a£
6.) Sampler's Name: t
7 ,) Evacuatio11 Method: ___ Bailer ___ Airlift Pump ___ Bladder Pump A _ Other
8.) Samplin1: Method: ___ Bailer ___ Bladder Pump ___ ID Number
I 9.) Field Ob.servatiollS and Sampling Co11ditio11S
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Outside Temperature: 1, !) 9.1)
9.2)
9.3)
W cather ConditiollS: Clear
(."q
__ Cloudy Calm
No
_L.No
__ W-mdy _2(__R.ain
Was the well locked upon arrival?
An)I unusual co11ditio11S in the area?
__x__ Yes
Yes
If "Yes" explain; _______________________
_
10.) Well Evacuation (all measurements are referenced from the top of tho well casing)
10.1) Casbg Diameter (ID): ;;/ • //I) (mches)
10.2) Total Well Depth: /, I • [i0 (feet)
10.3) Stati.c Water Level: 2-1 • 5i I (feet)
10.4) Hei1;ht of Water Column: --5.i_. I~ (feet) (10.2 -10.3)
10.5) Wa.lJ.:r Volume in Well: ---k_ .. 21 (Ute~GB.
10.6) Evacuate _L. c@ Well ·Vo~ Prior to Sampling
10.7) Evacuate~-12]) (Liters/~) Prior to Sampling (10.6 "' 10.5)
Time Evacuation Started / 3 : / 6 (Use 24 Hour Time)
Time Evacuation Completed _LL: 3 ;, (U~our Tune)
10.8) Acturu Volume Evacuated----"~-=-· ..L,Y'J (liters/~)
10.9) Did tl1e well go diy'I ___ Y cs _X __ No
A) T'mte well went dcy )/4t : Date ~
B) Tune well Wll3 sampled I 3-_ :-Z,~'{-Date _:::_-=:_=:...,1:::~-::-_ --
q To!1u time between evacuation and sampling ___________ (Hours)
11.) Grou11dwater Elevali011
11.1) Surveyed Well Elevatio11 (MSL) c-,-______ (fect) Data Not Available_-:_-:: __
11.2) Static Water Level 'l. I ,ll (feet)
11.3) Static Water Elevatio11 (MSL) _________ (feet)
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Well ID __ 0.c.......::...G_--'----0/_
12.) Well S,unpling Da~,
12.1) Sample Collected
Test Parametera Bottle Typo
1oc iii r,
'i"/..~l'J VtoJ
..
Size Preservative Number Collected
I{!\. .. I fl,< /J. I -:J
~uvJ J/1 I 3
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I 12.3) Sample Appearance: .1-, Clear ___ Sediment Turbid ---12.4) Samples placed on ice immediately after collection.: _x__ Yes -, No
I 13.) Field Analyses
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Parametei~
Temperature (''C)
pH
Conductivi~r
(uS/cm)
Types of pH Buffers Used:
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Calibration Std.
NIA
if.C> (-, ,D
/15Z>D
4.0
7.0
10.0
Sample Reading
11,o
r::;' (,1
l~4
Lot Number ______ _
Lot Number ______ _
Lot Number ______ _
Std. After Sample
NIA
~A7
I ui,1)
10
2
060
Well ID 3
I 14.) Purge Summary
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Date & Time 3(€ Q<( ~lli:! ,: ib
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Volume Purged J:,,-lt. 1 11 UJ4J /JJ-0.
Well Temperature
i• 0, z_ /~. I Jo.)_ 1J), & /1,J ("C)
Well pH Reading /o, II 5,91 S"1fnq t;, b1 c;, ~b
Conductivity i~o /~D JL/4 {t./1/ ;V~ (uS/cm)
' '
Other
Remarks
15.) Well socured •mth lock after sampling? _::;I_ Yes
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No
16.) I, the undersigned, h=by certify that all of the above information is aecurate.
Signature _~CJ=1/M""--'Ll.,.......J L-"""-~ ~--Date----"'--3~/r:,-'--"/q<;"' __ r I
NOTE: Certain information {such as well elevations and mean sea level heights of well casings) ·cannot be
filled in on ,this form unless provided to IEA personnel by the clienL
d:\mise-frm\gmdwt.wp
10 061
11 !.!?/c~pany
I GROUNDWATER FIELD SAMPLING DATA SHEET
!EA, INC.
I.) Client Name: _ .... /.li~D=e~L=h~s~f~~Lt~e~/4 ... a..,11..,_(,'-"~t~-------------
2.) Client Location: SJe/6,!/ / NC
3.) Date: -~3-t-(f+-(4._~--
4.) Well ID Number ___ 6_6_'___,j'-q-'--___ 5.) Sampling Sequence It: ---"'f'-"6'-----
6.) Sampler's Name: --J,,,C..µ.,b,,...ois._0"""-"-1.J..llJlau,J1~ __ :7'_1mLLI.· -'-, 12-~-J(};r,""'-!=----
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7 .) Evacuaticm Method: Bailer ---___ Airlift Pump
___ Bladder Pump
___ Bladder Pump
ID Number
---,/-~Other
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8.) Sampling Method: ___ Bailer ---
9.) Field Obs:rvations and Sampling Conditions
9.1) Outside Temperature: __ _,_1__.0"--_("C)
Weather Conditions: Clear Cloudy Calm
No
...Jf..__ No
__ Ww.dy L_Rain
9.2) Was· the well locked upon arrival?
9.'.3) Any unusual conditions in the area?
_Ji_ Yes
Yes
If "Yes" explain: _______________________
_
10.) ·well Evacuation (all measurements are referenced from the top of the well casing)
10.1) Casin.g Dlametcr (ID): J . tJ» (inches)
10.2) Total Well Depth: ~@ (feet)
10.3) Statfo Water Level: 1, 0 • ')..1.--(feet)
10.4) Heigilt of Water Column: jf . 1\/'. (feet) (10.2 -10.'.3)
10.5) Water Volume in Well: --~"c-. 0 5 (U~~
10.6) Evacuate 3 . P12 Well -Volumes Prior to Sampling
10.7) Evacuate /l) . lfD (Litcrs!G~ Prior to Sampling (10.6 • 10.5)
Tune Evacuation Started /' :_JQ_ (Use 24 Hour 'Iime)
Tune Evacuation Completed / 3 : Jo (Use ~our Timo)
10.8) Actual Volume Evacuated fa ,:TV (liters/~) .
10.9) Did tb.e well go dty'I ' Yes ;,< No
A) Tune well went dry @:_--=_ Date
B) Tun,, well was sampled /:, . : 3 O Date -J.~/-9(+9-S:: __ _
C) Total time betwec.n evacuation and sampling (Hours) -----------
11.) Groundwater Enevation
11.1) Survey,:d Well Elevation (MSL) _______ (feet) Data Not Available
11.2) Static Water Level 1D.1,t, (feet) ----
11.3) Static Water Elevation (MSL) _________ (feet)
d:\mi ,c-f rm\gmdwt. wp
10 062
I Well ID
12.) Well Sampling Da~,
12. l) Sample O:>llcctcd
Test Parameters Bottlo Typo Size Preservative Number O:>llccted
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12.3) Sample Appearan= >( Clear ___ Sediment ___ Turbid
12.4) Samples placed on ice immediately aft.,,-collection: _1 Yes No
13.) Field Analyse::
Parameter
Temperature ('C)
pH
0:>nductivity
(uS/cm)
Types of pH Buffers Used:
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Calibration Std.
NIA
4.C> (,,C>
'
I lS75n
4.0
7.0
Sample Reading
1,(,1
~,!./~
,~~
Lot Number ______ _
Lot Number -------
10.0 Lot Number -------
Std. After Sample
N/A
ln,q1 ,
( v1Jb
10
2
063
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Well ID
14.) Purge Summary
Date & Time ?Ji q_<; -j7{;) .
/1 Ill I?:> &
Volume .Purged D,lt. 1--y ~ /Dr-.j A:1'
I
Well Temperature l/11, 5 n,1 µ,/ 2 I, I 2-/, I/ (°C)
Well pH Reading 5,1l 51S1 tj'-{L{( c:;, ¥3 t;,L//
Conductivity
I \ I AL t5? /ft, g' /fo I (uS/cm)
' Other
Remarks
· , 15.) Well secured with lock after sampling? ---:i':-Yea No
16.) I, the ilnders.igned, hereby certify that all of the above information is accurate.
Signature __ C~ ____ v Jg~(i;'..-' -
NOTE: Certain iio.formation (such as well elevations and mean sea level heights of well casings) cannot be
filled in <>n this form unless provided to IEA personnel by the clienL
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10 064
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An Aquarion t::Ompany
GROUNDWATER FIELD SAMPLING DATA SHEET
!EA. INC.
1.) Client Name: _ .... lfi-o=e~c~h=.s_f~Lt~t.=la.........,11c..,..(~Stf~------------
2.) Client Location: S!te/6 I.I ' Alt
3.) Date: __ .,,..}'-'-(-'-+y l-'t-'--6 _rf
4.) Well ID Number __ ___,,0'--'D...__·----<-2,_,5'c.......,,_--5.) Sampling Sequence /I: -~1-~---
6.) Sample.:'s Name: __ _...,(.µ,bR ...... is._0......,.,.uf-U.Jlec.wl~--(jWY/<.LJ... ,__,Plu~1 ...... ru±.....__ __ _
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7 .) Evacuation Method: ___ Bailer ___ Airlift Pump ___ Bladder Pump ~K~~Other
8.) Sampling Method: ___ Bailer ___ Bladder Pump ID Number ---
9.) Field Observations and Sampling Conditions
9.1) Outside Temperature: i-o (."C)
Woather Conditions: Clear __ Cloudy Calm _Wmdy --.l<-,-Rain
9.2) W:,s tho well loclced upon arrival? -!i--Yes No
9.3) Aily unusual conditions in the atea? Yes _L_No
If "Yes' explain:
10.) ·well Evacuation (all measurements a:re referenced from tho top of tho well casing)
10.1) Casing Diameter (ID): 8 . /lb (mches)
10.2) Toi.al Well Depth: 1', .--®.__ (feet)
10.3) Static Water Level: 7, I . D$ (feet)
10.4) HeightofWeJ.er Column:~_.__j,£__ f, ) (10. -10.3)
10.S) Water Volume in. Well: -~ Cf te allo
10.6) Evacuate ,3 . @ ell -Volumes or '"~~~:ling
10.7) Evacuate f . QD ~Gallons) ~or to Sampling (10.6 • 10.S)
Time Evacuation Started . / 1 : G S (Use 24 Hour 'lime)
Timo Evacuation Completed _ / 3 :~se 24 Hour 'lime)
10.8) Actual Volume Evacuated <? . c:/l) -,~---::,'Gallons)
10.9) Did tho well go dty'l _-,-.,._,..Yes ___ ~_No
~~~-~N&,___ ~-~~---
B) Tune well was sampled /) : 0 t( Date __ :!,..,l~s .. la'I-'-( __
C) Total time between evacuation and sampling __________ \~( ____ (Hours)
11.) Groundwater Elevation
I I. I) Surveyed Well Elevation (MSL) ________ (feet) Data Not Available ___ _
I 1.2) Static Water Level '1-1 , OS' (feet)
I 1.3) Static Water Elevation (MSL) -(feet) --------
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Well ID _ _cbc....=-b_' i_t{ __
12.) Well Sampling Dain
12. I) Sample Collected
TC-'t Parameters Bottle Typo Size Preservative Number Collected
/J OL I/ I r.P I) o ... ; ~1(0u j
'
12.3) Sample Appearance: . A Clear ___ Sediment ___ Turbid
12.4) Sampks placed on ice immediately after collection:_)_ Yes No
13.) Field Analyses
Parameter
Temperature ("C)
pH
Conductivity
(uS/cm)
Types of pH Buffors Used:
d:\mi~-frm\gmdwt.wp
Calibration Std.
NIA
i+.o /,.o
'
I r;m--,
4:0
7.0
10.0
· Sample Reading
/JI'•
ln.11.i
~i.
Lot Number ______ _
Lot Number -------Lot Number ______ _
Std. After Sample
NIA
~.17
I ,mri
10
2
066
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Well ID
14.) Purge Summary
Date & Time
Volume .Purged
Well Temperature
(°C)
Well pH Reading
Conducfr,ity
(uS/cm)
Other
Remarks
3/~/~(
11~{
L,J+.
1-1 ,)
~ .~i.-
~4
j/f~ -,3 .
3 & ¥& f f,,
20,</ /f, I /7. ~ /7, 1
'
In .'31 It;, 1-i lo, 2i ~. I1
~J_ /,, r; GJ lo)
I , , 15.) Well secured with lock after sampling? -2.{_ Yes No
I 16.) I, the undersigned, hereby certify that all of the above information is accurate. ·
Signature
NOTE: Certam information (such .. well elevations and mean sea level heights of well =ings) caruiot bo
filled in on this form unless provided to IEA personnel by the client.
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I 10 067
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M Aquarion Company
GROUNDWATER FIELD SAMPLING DATA SHEET
!EA, INC.
I.) Client Name: --+-//i ..... o,_,,e_,_e,,.,_h=5'-'-f_Ci .... t. .... /4Cld.L-ou.f .... .S ... t ____________ _
2.) Client Location: SJel6J 1 NC
3.) Date: --3..,...(r ...... f q-( __
4.) Well ID Number M /4 -5 4 5.) Sampling Sequcnco U: __ 7,.-:;...:;_Z, __ _
6.) Sampler''s Name: __ ..,.,(..,µ,bLJU,ais.....__,_,d'-"-vtLIJIACLIO!~"---¼m"""·L!..!-,.....,61~
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7.) Evacuatfon Method: ___ Bailer ---Airlift Pump ___ Bladder Pump
___ ID Number
_...X_-Other
8.) Sampling Method: ___ Bailer ___ Bladder Pump
I 9.) Field Observations and Sampling Conditions
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Ou1:side Temperature: --~/ 6-1? ___ ('C) 9.1)
9.2)
9.3)
We1thcr Conditions: Clear __ Cloudy Calm
__ No
__ Wmdy _:f,_R.ain
W "'' the well locl<ed upon arrival?
Any u.o.usual conditions in the area?
_L Yes
Yes _L_No
If •y cs" explain: --,-----------------------
10.) · Well Evacuation (all =eats IU'C referenced from the top of the well casing)
10.1) Casing Diamclcr (ID~:. (,lll (mchcs)
10.2) ToU!I. Well Depth: 'S • Q]J (feet)
10.3) Static Watu Level: 3 . lie (feet)
10.4) Height of Water Column: · !f . 6 ~ (feet)~l0 -10.3)
10.5) WatJ.,r Volume in Well: _ _.!3a._• £7 (Li.ten/ allo · .
10.6) EvacWlte 3 . Ob Well Vol~ Prior to ling
10.7) Evacuate x'. • /Jj) (Uter&'G~ Prior to Sampling (10.6 • 10.S)
Time Evacuation Started d : 15' (Use 24 Hour Time)
TLme Evacuation Completed _____i!:/__: 3s' (Use 24 Hour Time)
10.8) Actua:l Volume Evacuated NiJl5 (Uters[~
10.9) Did tho well go dry7 ___ Yes y No
A) Tm10 well went d,y iA bf =---,-Date /-
B) Time well was sampled¼ /f . 3 > . Dato ::>_/...,~~/,+-¢'{' ___ _
C) ToM time between evacuation and sampling · 7 (Hours)
11.) Groundwater Elevation
l I. 1) Surveyed Well Elevation (MSL) _______ (feet) Data Not Available
11.2) Static Water Level 3X,f\Q (feet) ----
11.3) Static Water Elevation (MSL) _________ (feet)
d:\misc-frm\gmdwt.wp
10 068
12.) Well Sampling Data
12. l) ~:ample O,llected
Test Parameters Bottle Typo Six.e Preservative Number O:>llected
~\ Cl lf 1 (, 'j{)wJ U,(~,1 i
~i'iD 1]/(1 4D I'>.~
0 3 f.l l \
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12.3) Sample Appearance: . 7S, aear ___ Scdimc.nt Turl>id ---
12.4) Samples placed on iee immediately aftQ' collection:~ Yes No
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13.) Field Aaaly":s
Parameter
Temperature ("C)
pH
O,nductivily
(uS/cm)
Types of pH Buffers U~:
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Calibration Std.
N/A
4.C> f,.D -·
•
l15lSD
4.0
7.0
10.0
Silniple Reading
I ,1. 4
c:; 11 i./
~4~
Lot Number ______ _
Lot Number ______ _
Lot Number -------
Std. After Sample
N/A
~.~1
, ,mn
'
10
2
069
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14.) Purge Summary
Date & Time ?7(~ ~ , fff(!r
/l (fl ,~ 7:JC: .
Volume Purged · Lf'l+. 3 (v ~ ()f\\
Well Temperature 7r,', I (3;°! I
(°C) /<.j,3, I✓ l/
Well pH Reading ; 's-<o <;. (/3 i,t12 c:;q~
Conductivity 3sq 3?< 7:ilf-1 3<1< (uS/cm)
Other
Remark,
·. \ 15.) Well SCCUIC<l with lock after sampling? _.2:_ Yes No
3
A hA
/7,i
'?1 t 2-
-slfl
I 16.) I, the undersigned, hereby certify that all of the above information is accurate.
Signature --->---'---(Jv1vo-=---b-!2~A-~'-"----~-Date 3k/2c __ ....,.(_( ____ _
NOTE: Certain information (such as well elevations and mean sea level heights of well casings) ·cannot bo
filled in -on this fonn unless provided to lEA personnel by the clienL
d:\misc-frm\gmdwt.wp
10 070
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NI AQu<uion Company
GROUNDWATER FlEU) SAMPLING DATA SHEET
!EA, INC.
I.) Client Name: -➔lli..uD.,_,e,_,c"'"'h_,,cS::..;f'--
.
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.... aLU.Jl..uS"t~-------------
2.) Client Location: ---'S.....,..Je ...... li .... i.!f,,_._, _,_M..,_'C=--------------
3.) Date: __ ___;J.µl't4-!1'-'-t( __
1
( ( i?JGO ~ //-Z 3, 5.) Sampling &quenco II: _ __::1_,?:__ __
6.) Sampler's Name: ------1C...4.h.uuR1$.>.....\..LO..lll.vt.llllaw..1i' _(l.a.,'./4maL· ~6"-"'Wr1-1-"J="--. ---4.) Well ID Number
7.) Evacuation Method: ___ Bailer ---Airlift Pump
___ Bladder Pump
___ Bladder Pump
___ ID Number ·
;< . Other
8.) Samplin;g Method: ___ Bailer
9.) Field Observations and Sampling Conditions
9.1)
9.2)
9.3)
Outside Tempernb.lre: __ ___:.;f fy"'-__ ("C)
Weather Conditions: Clear Cloudy Calm __ Wmdy
Wes the well locked upon arrival? ~ Yes No
..L_Rain
A11y unusual conditions in the area? Yes -L.. No
If "Yes• explain:--'-~---------------------
{)@e {f]1 m,» !eftik.
10.) Well Evat:uation (all measurements are referenced from the top of tho well casing)
10.1) Ca:rlng Diameter {ID): Q . (JD (mches)
10.2) TCltal Well Depth: :Z. ', • 1ft, (feet)
10.3) Sbllic Wa!r.r Level: /( • 9'; (feet)
10.4) Height of Wair.r Col= I { _._!fl_ (feet) (10.2 -10.3)
10.5) W:ur,r Volume in Well: --"--"....:ff.JL_ (Lltets/~
10.6) Evacuate±· @ Well Volumes Prior to °§impling
10.7) Evacualc • lJ!J (Litots/~ Prior to Sampling (10.6 • 10.5)
Time Evacuation Started / { : 'i> (Use 24 Hour Time)
T"une Evacuation Completed l'i : 7f (Use ~ur Time)
10.8) Aci.'ual Volume Evacuated lo Q7l (Utets/G~
10.9) Ditl tho well go d,y'I __ ~ Yes i,, No
A) 11me well went dcy Mf-:.___ Dato / ,
B) 1ime well was sampled f4. : IS: Dato '.;> ?/~ 2
C) 1otal time betwee,i evacuation and sampling _______ 1 _____ (Hours)
11.) Groundwat<>r Elevation
11.1) Surveyed Well Elevation (MSL) ______ (feet) Data Not Available--==--
11.2) Stati.c Water Level /1,93 (feet)
11.3) Static Water Elevation (MSL) ___ -____ (feet)
10 071
I Well ID
2
12.) Well Sampling Dau,
12.1) Sample Collected
.
Test Parameters Bottle Typo Size Preservative Number Collccte<l
1DG Ur. 'fW 1+.,__50-1 -z._,
~Zt/D I /1 r. l/OvJ /{Cl ~
f-f-i: t. (Jr;J l fl r, ~oJ 'f °c, 3
Vvl I' ~7/
.
1/1 (1 J Jn ,,, Q Wl'S/\ /.I ( ( 2.,
10 l V111V w, D V/C lf/) l,, f i/, (/)'c/ 2
ff/wfo,,.1 f;; "/wl ~!S1 u1h I !rt. Un,,,g ~
l.f-,' (... <;
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12.3) Samp.le Appearan= -:---_Clear __ Sediment _k__ Turbid
12.4) Sampl:es placed on ice immediately after collection: ---4-Yes No
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13.) Field Analyses
Parameter
Tempernture ("C)
pH
Conductivi~y
(uS/cm)
Types of pH Buffers Used:
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Calibration Std.
_N/A
4.C> /,.o .
/ l575'r)
4.0
7.0
10.0
-Sample Reading Std. After Sample
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-lo, o3 {;,q7
3¥~0 ,tr/Jl)
Lot Number _____ _
Lot Number ------Lot Number ------
10 072
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Well ID
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14.) Purge Summary
Date & Time ??/f/qs 3/y;lf(
,.c( /(' 1<
Volume Purged L,lt. i ~ ~r,1 I ,1)-/4,,
Well Temp-:rature
I
/ \t?; ,<,, ft, 0 /5, j 1,/6-0
(°C)
Well pH Reading <;, t z_ &. II (J,!( b-05 t,d3
Conductivity J..O/D 79ub 32-sD Ji/L/0 sY;a
(uS/cm)
Other ~
Remarks
15.) Well =red with lock after ~ling? _l_ Yes No
16.) I, the undersigned, hereby certify that all of the above information is accurato.
Signature ----l,.......L[jw.L--:l---f~ ~o ,Jl~· ,_
NOTE: Certain information (such as well elevations and mean sea level heights of well casings)·canaot be
filled in c,n this form unless provided to IBA personnel by the clienL ;
'.
d:\misc-frm\grndv.rt.wp
10 073
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_I_ .1-J J... >-
M Aquorion Company
GROUNDWATER FIELD SAMPLING DATA SHEET
!EA, INC.
1.) Client Name: _ _,_l/i.u.D,.,,eu.k<.!.h,,,.s~f_..,.(j""ec£.lla .... r1u....,(, ..... (t.._ ____________ _
2.) Client Location; [;Jp/ 6}/ ! NC
3.) Date: --~JH/q+-/9'--'S'--'--
l
4.) Well ID Number __ __,_(..,.(~--3'"-'j~---=--5.) Sampling Sequence #: -~2.~V __ _
6.) Sampler's Name: ---C-bo ...... is_,_d"-"vt"-'-l ...... a:1;)...___1,=Iim.u......i.-6'""-'·k/-01 ..... J=---
7 .) Evacuatfon Method: ___ Bailer ___ Airlift Pump
___ Bladder Pump
___ Bladder Pump
ID Number
--<>-~Other
8.) Sampling Method: ___ Bailer ---
9.) Field Ob!:ervations and Sampling Conditions
9.1) Outside Temperature: ----'~--("q
Weather Conditions: Clear __:i._, Cloudy Calm
9.2) Wa, the well locked upon arrival? ___;f_ Yes No
9.3) Any unusual conditions in the area? Yes -X.-No
If "Yes' explain:_-'-----------------------
__ Windy Ra.in
I 10.) · Well Evacuation (all measw=ents are refe:cnced from the top of tho well casing)
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10.1) Casbag Diameter (ID): J. . 6D (mches)
10.2) Total Well Depth; __Ji_._ DI) (feet)
10.3) Stali.c Water Level: ---1:1:,_. ID (feet)
10.4) Hei1:ht of Water Column: /o . q (J (feet)(l0.2 -10.3)
10.5) Wa!i,.r Volume in Well: _ _,__. 71 (Liters/~)
10.6) Evac,uate ±· @ Well Volumes. Prior to Sampling
10.7) Evacuate . • (:]) (Liters/~ Prior to Sampling (10.6 • 10.5)
Time Ev~on Started r g : , W b (Use 24 Hour Tune)
Time Evacuation Campi~ '1 : ell (Uso 24 Hour 'l)me)
10.8) Actual Volume Evacuated (, • O (Uters/Gall"jii))
10.9) Did tb.e well go dry? ___ Yes ;x' No
A) Tm1e well went dry A! Ir: Date
B) Time well ws:i sampled u-~--,--r1 Date -=-~3-t:,/'--''1:/7°2_\:_• =-=-=--
q Tetu time between evacuation and sampling ___________ (Hours)
1 I.) Groundwater Elevation
11.1) Surveyed Well Elevation (MSL) _______ (feet) Data Not Available ___ _
11.2) Static Water Level 1-'J-1lQ (feet)
11.3) Static Water Elevation (MSL) -(feet) --------
d:\misc-frm\gmdwt.wp
10 074
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Well ID
12.) Well Sampling Data
12.1) Sample Collected
Test Param.eter:1 Bottle Typo
10G \Jlo.Y._
g'.LiO ,rtflv
Size
~01..J
40,J
2
Preservative Number Collected
H,SOJ j
V
/./Ci 3
12.3) Sample Appearance: / Clear ___ Sediment Turbid ---
12.4) Samples placed on ice immcdiatcly after collection: ...:i,.__ Yes No
13.) Field Analyses
Parameter
Temperature (0 C)
pH
Conductivity
(uS/cm)
Types of pH Buffer:, Used:
d:\mi~-frm\gmdwt.wp
Calibration Std.
NIA
4.6 f,.D .
Jr::m--.
4.0
7.0
10.0
Sample Reading
/7.o
~,. 71
~/D
Lot Number -------Lot Number ______ _
Lot Number -------
Std. After Sample
N/A
J./)7)
qqq
10 075
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Well ID CJ ... · 3? 3
' ' ,4.) Purge Summary
Dale & Time '.)~ lq~ "3(1(1 (
CS'-lb /)q (7.,
Volume Purged L,Jt. ,.., ~ ' ~ D Hr1 1--lr C1(, ·
Well Temperature ;{) I , . 1:,{ 17,0 !
(·C) ' 0 ,7 11.7--
Well pH Reading I I') L 6 3 t. 7d &.71 ?, 10 ,1' °'\
Conductivity 111 }57 Li'OZ 4/0 411 (uS/cm)
Other
Remarb
•. , 15.) Well secured with lock after sampling? ...:£_ Y cs No
16.) I, the undersigned, hereby certify that all of the above information is accutate.
I I
Date J.i'J;7 ( ----------
NOTE: Certain information (such as well elevations and mean sea level heights of well casings) ·cannot be
filled in c,n this form unless provided to IEA pe=nnel by the client.
d:\misc-frm\g:rndwt.wp
10 076
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....._..._....,.__ M AQu:>rion C,mpany l
GROUNDWATER FIELD SAMPLING DATA SHEET
!EA. INC.
1.) Client Name: _....,//i....,_._/)'-"'~--'""'h-'s=-f_.,.Cc,.e'-.Lla.l"-Lo.w!u.,~ ... t:._ ______________ _
2.) Client Location: --~S,,_,Jwec..t./ilL~,y-'f--i,-'-M'-'C."'-----------------
3.) Date: ---'~'+'sf+-1[9::.-~ _
4.) Well ID Number ___ .... W,._.""---l,P--'cc""'"''"----"~L..41..-5.) Sampling Sequence /I: _ .... z'--'~"----
c b . (j l/ "' :c y,y: ,J.
6.) Sampler"s Name: __ ___,__,_,uRut<._,_..,_..:...ll.llJ[.JJArulALAJ __ 0
u,IYt1.ru_,_l)..d.Q.:.,1=tl!id._=-------
7.) Evacuati,,n Method: ___ Bailer ---Airlift Pump
___ Bladder 'Pump
___ Bladder Pump
___ ID Number
·y' Other
8.) Sampling Method: ___ Bailer
9.) Field Ob,:ervations and Sampling Conditions
9.1)
9.2)
9.3)
Outside Temperature: ____ .,~,....__ (."C)
Weather Conditions: __ Clear __;1,_ Cloudy
Wa., the well locked upon arrival? -+ Yes
Any uausual conditions in the area? Yes
Calm
No
._:i_No
__ Wtndy
If 'Yes' explain:--'-----------------------
10.) · Well Evacuation (all measurements arc referenced from the top of the well ca.sing)
10.1) Casing Dia.meter (ID): /}., • (JJ (tnches)
10.2) Toti! Well Depth: la 4 ._j)J2__ (feet)
10.3) Static Water Level: tlJ _._:il_ (feet)
10.4) Height of Water Column: /J J.!. • C'J (feet) (10.2 -10.3)
10.5) Wator Volume in Well: J' 1• /1 (Liters/~~) ·
10.6) Eva<:wtte 3 . t:11) Well -Volumes Prior to "Sampling
10.7) Evac:uate -:J.} • Cb (Lite~G~ Prior to Sampling (10.6" 10.5)
Time Evacuation Started l'f: (Use 24 Hour Time)
. Time Evacuation Completed 09 : 3c (Uso~our Tune)
10.8) Actutl Volume Evacuated 2 7 . ~1' (Liters/~)
10.9) Did the well go dry? . Yes ;( No
A) Tune well went d,y QI,: Date ,,.,....i-,' ~---
B) Time well was sampled (Ji.: :itl Date ~/j/q?
C) Total time betwee.n evacuation and sampling ______ 1_, _____ (Hours)
1 !.) Groundwater Elevation
1 I. 1) Surveyed Well Elevation (MSL) _______ (feet) Data Not Available ___ _
11.2) Static Water Level lq,C\J (feet)
11.3) Static Water Elevation (MSL) _________ (fcel)
d:\misc•fnn\gmdwt.wp
Rain
10 077
2
l2.) Well Sampling DalA
12. I) Sample Collected
Test Parameters Bottle Typo Siz.c Preservative Number Collected
TOG \)/Cl.!l 4tlrJ 1LSD4 8-
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12.3) Sample Appearan= ')( Clear --,,-....,. Sediment Turbid ---
12.4) Samples placed on ice immediately after collection: --1,.._ Yes No
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13.) Field Analyses
· Parametex·
Temperature (°C)
pH
Conductivity
(uS/cm)
Types of pH Buffers Used:
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Calibration Std.
NIA
if.C> /-, ,D
'
/ l'v'SI")
4.0
7.0
10.0
Sample Reading
/') ~
ifl 1&
71
Lot Number -------LotNumber -------
Lot Number -------
Std. After Sample
NIA
7. <fl)
~qg
10 078
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,4.) Purge Sum.m:uy
Date & Time
Volume Purged
Well Temperature
("C)
Well pH R,,ading
Conducti'tity
(uS/cm)
Other
Remarks:
'~ h >
IV) "l,~
L,t.
/ 3 .i
~:,l ~
:. I
~!:
1 /4 JZu,.V I. i h A
Cl 0
I b ,~ /3J I½•~ /b, 1
,,Sb 1,og / .. ,1& i.:, li
5J.. 3°1 ?f) ·yi
I ·. , 15.) Well secured with lock after sampling? -,l(..._ Yes
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No
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16.) I, the undersi,gned, hereby certify that all of the above information is accurate.
NOTE: Certain information (such as well elevations and mean sea level heights of well casings) cannot bo
filled in 011 this form unless provided to IEA personnel by the client.
d:\misc-frm\gmdwt.wp
3
I 10 079
1 Dr\..
I.) Client Name:
2.) Client Location:
3.) Date:
4.) Well ID Number
6.) Sampler's Name:
GROUNDWATER FIELD SAMPLING DATA SHEET
IEA, INC.
iloee,hsf Celcio~1e
. SJel6:;, NC
?h/c;5:
K-a~ 5.) Sampling Sequence#:
(.bR,S ddlfHJ 1k~J
1
:Z.le
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I 7 .) Evacuation Method: ___ Bailer ___ Airlift Pump ___ Bladder Pump
ID Number
'{ Other
8.) Sampling: Method: ___ · Bailer ___ Bladder Pump
I 9.) Field Ob:;ervations and Sampling Conditions
'7
Outside Temperature: ---""--__ (."q
---
9.1)
9.2)
9.3)
Wc:ather Conditions: Clear _x.,_ Cloudy Calm
Was the well locl::ed upon arrival? ~ Yes No
__ W-mdy
Any unusual conditions in the area? Yes _j__ No
If 'Yes' explain:-'------------------------
10.) ·well Evacuation (all measurements are referenced from the top of the well casing)
10.1) Casfng lliaJnetcr (ID): a.~o (1nches)
10.2) Total Well Depth: ~X . (feet)
10.3) Stalic Water Level: II . (feet)
10.4) Height of Water Column: I l• • ,,(p (feet) (10.2 -10.3)
10.5) WaJ'r-r Volume in Well: :Z.. lR I (Iit.ers/G~
10.6) Evacuate 3 . ITT> Well Volumes Prior to Sampling
10.7) Evacuate g'. • {[[) (llt.ers/~rior to Sampling (10.6 * 10.5)
Time Evacuation Started / Z... : :,1, (Use 24 Hour Time)
1ime Evacuation Completed j'J, : 2 D (Use 24 Hour Tune)
10.8) Act1.tal Volume Evacuated ~ 0) (Ut.ers/Gat!§JO
10.9) Did the well go dJy'l _ _,.,._Yes ;{ No
A) Timo well went d,y /J.A Date
B) Tune well wu sampled 11 . : ')D Date 3="'/""li +(q-S:: __ _
q Total time between evacuation and sampling ____________ (Hours)
11.) Groundwatel' Elevation
Rain I
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I I I. I) Survc,yed Well Elevation (MSL) _______ (feet) Data Not Available
11.2) Static Water Level /(,qq (feet) ----
11.3) Static Water Elevation (MSL) ___ -_____ (feet)
d:\nusc•frm\gmd-.wt.wl_)
080
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Well IO ____.K~~ _?J_1 __
12.) Well Sampling Dall\
12.1) Sample Collected
Test Paran1etcrs Botllo Typo
1(1:, vu!
X'J..lft, ,1 ,r, ~
Size
LfOr • .Q
~OtJ
12.3) Sample Appearance: X Clear ___ Sediment
Preservative
~. ~Dll
Llr I
Tumid ---
12.4) $am,?les placed on ice immediately aftct-collection: -,\.-Yes No
Number Collected
()
3
I 13.) Field Analy,:cs
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Parameti~
Temperature (°C)
pH
Conductivity
(uS/cm)
Types of pH Buffers Used:
d:\misc-frm\gmdwt.wp
Calibration Std.
. N/A
4.c> /,.o .
I /S]57-)
4.0
7.0
10.0
· San:iple Reading Std. After Sample
/1,;, I NIA
~ (,;Cj '7.lil--
7,.. '71 Cf/9
Lot Number -------Lot Number -------Lot Number -------
10
2
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,4.) Purge Summary
Date & Time '3/q q~-->/1/-15
I LJ:>t -t:25u
Volume Purged ]::Nt. 3 0 q/1/i; 41-k1
Well Temperature 15,2 /5,5 JS, LI ti I I 7{,;
(·C_I
Well pH Reading 6 ,i-1{ ' t, 61 6. 65 f Zc7 6,59
Conductivity L//J lfi6 )S7 ~77 30</ (uS/co1)
Other
Remarks
-.. \ 15.) Well secured with lock after sampling? _L_ Yes No
16.) I, the undersigned, hereby certify that all of the above information is accw-atc.
NOTE: Certain information (such as well elevations and mean sea level heights of well casings) cannot bo
filled in, on this form unless provided to IEA personnel by the clienL
d:\mise-fcm\gmdwt.wp
3
10 082
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M A.Quarion C.wnp:my
1.) Client Name:
2.) Client l..oc.ation:
3.) Date:
GROUNDWATER FIELD SAMPUNG DATA SHEET
!EA. INC.
//Dech.sf Celaa,.st
SAd6u, NC
,-;
?J/c,/q1<
1
4.) Well ID Number ~-~~ 5.)
C.bois Ovt:IM~
7g Sequence II: _..:;;1..._J...,_ __ _
im &1ai±
6.) Sampler's Name: {
7.) Ev.acu.ation Method: Bailer ---__ ,...Airlift Pump
___ Bladder Pump
___ Bladder Pump
___ ID Number
-"X'--~Other
8.) Sampling Method: ___ Bailer
9.) Field Ob,;ervations and Sampling Conditions
9.1) (MsidcTomporature: ____ 1-__ (.'C)
Wc:ather Conditions: Cloar __l_ Cloudy Calm
9.2) Was tho well lockod upon anival? _i._ Yos No
9.3) Any unusual conditions in the area? Yos ---t--No
If 'Yos' oxplain: --,----------------------,--
__ Windy Rain
10.) ·Well Evacuation (all measurements are referenced from the top of tho well casing)
10.1) Casing Diameter (ID): J . OI) (me.hes)
10.2) Total Well Depth! 5$ . l O (feet)
10.3) Static Water Level: I~ . D ', (feet)
10.4) Height of Water Column: ·./II • b] (feet)(l0.2 -10.3)
10.5) Wa.1:er Volume in Well: 7 . / /4 (Liters/~)
10.6) Evacuate 3 . p:p Well Volumes Prior to Sampling
10.7) Evaouate 'J, 1--• cJI) (l.iters!aG} Prior to Sampling (10.6 "' 10.5)
T'imo Evacuation Started /t-: Z.. C (Use 24 Hour Time)
Time Evacuation Completed /~ : 6J (Use 24 Hour Timo)
10.8) Acttw Volume Evacuated 1.,1, . 6D (Liters/~
10.9) Did tho well go dry? ___ Yes _._ __ No
A) Timc well went dry Ml, =,----Date
B) Ti1ne well was s:amplod I~ . =~®~-Date -3-,-~..,/<j-.5'..,,.... __ _
C) Total time between evacuation and sampling ------~! ____ (Hours)
11.) Groundwater Elevatio11
11.1) Survc·yod Well Elevatio11 (MSL) ..,... ______ (feet) Data Not Available
11.2) Static Water Level 14,01 (feet) ----
11.3) Static Water Elevatio11 (MSL) ___ -_____ (feet)
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10 083
Well ID
12.) Well Sampling Daln
12.1) Sample Collected
Test Parameters Bottlo Typo
!OG \J t&
Size Preservative Number Collected
t!oJ 1-LS04 ;..
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I 12.3) Sample Appearance: )( aear ___ Sediment Turl>id ---
12.4) Samples placed on ice immediately after collection: -A-Yes No
I 13.) Field Analyses
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Parnmete:r
Temperature (°C)
pH
Conductivit:1
(uS/cm)
Types of pH Buffers Used:
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Calibration Std.
NIA
4.C> / t-D .
l15Z5D
4.0
7.0
10.0
· Sample Reading
)'/,(
Y, 11
'12-ab
Lot Number -------Lot Number -------Lot Number -------
Std. After Sample
NIA
1,(5[)
qqq
10
2
084
I Well ID __ ..1..k,__-..:.6..:.~--3
I ( ... 4.) Purge Summary
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3/q/q; ;/q/qs .
Date & Time
11. 1 " l4nQ
'
Volume Purged :[j-[t. 7 fl/. ttc:nd 4¼J
I l Well Temperatui,, 15.I /(, ~ ;c;,o /~,5 /,; 14 (°C)
~ e
Well pH Reading 1/,67 "i,77 t-/, 75 t,f, 7c1 ~. 1 V7
-
Conductivity tJJtJO v/<;n 6110 0ioo C,21 D (uS/cm)
Other
Remarks
(:·
15.) Well secured ·with lock after sampling? _j_ Yes No
16.) I, the undersigned, hereby certify that all of the above information is accurate.
Signatul<> ~Lh_· ____;:()::;.._;;_~~--· · _ Date __ 34-(,J.1.9.f~9..,__< __ _
NOTE: Certain infonmtion (such as well elevations and mean sea level heights of well casings) cannot be
filled in on this form unless provided to IEA personnel by the client.
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10 085
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•' !E;l~any l
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GROUNDWATER F!EU) SAMPLING DATA SHEET
!EA, INC.
I.} Clical Name: --1-lli..u.0£.>eu.k<.!.h_,_,s~f'---..,.(t"-'-eu..lald..oL.UJ(,.uS:t,._
_
____________ _
2.) Clical Location; SJe/61 ' NC
3.) Date: _ ____::5-1-/q4-/q...,_5" __
l [
4.) Well ID Number -----'f_-...;5~~=------5.) Sampling Sequcace II: _ __:2-=-.)' __ _
6.) Sampler's Name: __ (L,...,bl.11'1<.l,.l.is _,_Qt!J/.vl:J....IJlaw.,W.1--_✓fT'--¼m=· _./2..:.o'4""4,f=41l.i.:i..f __ _
7.) Evacuation Method: ___ Bailer ---Airlift Pump
___ Bladder Pump
__ Bladder Pump
___ ID Number
_'/...,._~. Other
8.) Srunplin1: Method: ___ Bailer
9.) Field Observations and Sampling Conditions
9.1)
9.2)
9.3)
O11.tside Temperature: :Z..
W,:ather Conditions: Clear
W,,s the well locked upon arrival?
An_y unusual conditions in the area? .
(."q
___£){__ Cloudy
--X-Yes
Yes
Calm
No
J.._No
__ Windy
ff'Yes"cxpla.i.n:-'-......;...---------------------
10.) Well Evacuation (all measurcmcnts are ref=ccd from the top of thG wc!l easing)
10.1) Casing Diameter (ID): ct . iJb (mches)
10.2) Total Well Depth: 5:$ . 50 (feet)
10.3) Stal.ic Wattt Level: 1,0 . 5:l (feet)
10.4) Height of Wattt Colwnn: '3 / . C/ I (feet)(l0.2 -10.3)
10.5) Wat.r-r Volume in Well: 5 . 11 (Iltern!G@.i ·
10.6) Evacuate _3_. c@ Well -V~~Prior to Sampling
10.7) Evacuate __Jjp__. (JU (Utcrs/~rior to Sampling (10.6 • 10.5)
Time Evacuation Started Cfi :--2Q__ (Use 24 Hour Time)
Time Evacuation Completed ~!J~: ~ (U~ Hour Timo)
10.8) Actual Volume Evacuated /£ .QU (Uters!Q___a110rls)
10.9) Did the well go dry? ___ Yes ?<, No
A) Time well went d,:y ___ .___ Date _____ _
B) Tiine well was sampled / 0 . :._,'f..:.S__ Date Q S Q'l q_s
q Total time between evacuation and sampling __ 5"-S'_r-,,_~,·...._ _______ (Hours)
I I.) Groundwater Elevation
11.1) Surve:yed Well Elevation (MSL) ________ (feet) Data Not Available -
11.2) Static Water Level '.l-~ 81 (feet)
11.3) Static Water Elevation (MSL) ___ -_____ (feet)
d:\mis:e-fnn\gmdwt.W'(i'
Rain
10 086
Well ID __ P_-_6_'6 __
l2.) Well S:tmpling Data
12. I) Sample Collected.
Tc.st Parameters Bottle Typo Size Preservative Number Collected
foe 1Jir,U l/Drr1 ~L,o u ,.'.,l
i1-AD V1cJ. "tDw
-' ) 14 c. I
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12.3) Sample Appearance: ,,( Clear ___ Sediment Turbid ---
12.4) Samples placed on ice immodiately a&r collection: __l_ Yes No
13.) Field Analyses
Paramettr
Temperature (°C)
pH
Conductivity
(uS/cm)
Types of pH Buffers Used:
I d:\mis.c•frm\gmdwt.wp
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I
Calibration Std.
NIA
4.C> f-, -D .
l15Z>O
4.0
7.0
10.0
· Sample Reading
11,1...-
fn In ~
rf/1
Lot Number -------Lot Number -------Lot Number -------
Std. After Sample
NIA
1.ob
m
10
2
087
I 3
I '·· 14.) Purge Summary
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Date & Time J/4 qs' )19 ~~
('j 1t;D .. ; IOY -
'
Volume Purged Lt'+. c; /D //p 1~,J /4 /1r0
Well Temperature
(°C) It, Z, 1gs I 7, 1 /7,-<, I y I I
Well pH Reading '7,D{ /, 15 bi5 {,(~ {6'}
•
Conductivity t./l,:L H-1~ t7t t?~ ?ri (uS/cm)
Other
Remarks
15.) Well secured with lock afw sampling? _L_ Yes No
16.) I, the undersi1~cd, hcceby certify that all of the above information is accurate.
NOTE: Certain information (such as well elevations and mean sea level heights of well casings) cannot be
filled in 011 this form unless provided to IEA personnel by the clienL
d:\misc-frm\gmdwt.wp
10 088
,~ !~lo! .. ~
I GROUNDWATER FIELD SAMPLING DATA SHEET
!EA, INC.
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I.} Client Name: _ _,_l/i_,..D...,e"""c"'-,h~.s"-'f-~0'-"e"-'la=t1~l~5t~-------------
2.) Client Location; SAe/6!/ J lie
3.) Date: -.cc.+3l-4-q /q'-'-> __
4.) Well ID Number ____ _,_,Af"---_1..:-'q--=---5.) Sampling Sequence #: ,----=2'--1-'----
6.) Sampler's Name: -----'CldJ.b-R ........ is ..,_Q<..:,<.vtJ..jJIPru..o,(;).,___/T=/4w,=· ~O=M(L-d~---
7.) Evacualion Method: --X-Bailer
8.) Samplmg Method: ---'-'X,-Bailer
---Airlift Pump
___ Bladder Pump
___ Bladder Pump
___ ID Number
. Other --~
9.) Field Observations and Sampling Conditions
9.1)
9.2)
9.3)
Outside Temper.,.ture: ----'1-,____("C)
Weather Conditions: Clear _..x. Cloudy
Was the well locked upon arrival?
Any unusual conditions in tho area?
--1._Yes
Yes
__ Calm
No
-1._No
__ Windy
U "Yes" explain: ------------------------
.10.) ·Woll Evucuati.on (all measu=ents are referenced from the top of tho well casing)
10.1) Casing Diameter (ID): ~ • t/l) (Inches)
10.2) 1otal Well Depth: __J,fL:_ O'o (feet)
10.3) Static Water Level: _L. 2, I (feet)
10.4) Height of Wat/or Colwnn: 7-D • 7~ (feet) (10.2 -10.3)
10.5) Water Volume in Well: · ll-'ii)'. ~allons)
10.6) Evacuate 3 . OJ? Well Volumes Prior to Sampling
10.7) Evacuate 3q . l[D <@!Gallons) Prior to Sampling (10.6 "' 10.5)
Time Evacuation Started // : Q () (Use 24 Hour Tune)
Tune Evacuation Completed ( ( :~se 24 Hour Time)
10.8) A·,tual Volume Evacuated · ~j . OI> _ ~allons) ·
10.9) Dro the well go dry? _...,.,._Yes ::,., No
A) Time well went dry N4 : ~ Date
B) 'lime well was sampled / /. : ?,5 Date Q'""}"'q-, "\-,""i,;,----
C) Total time between evacuation and sampling __ 2--'5'-"AJ.:J'--------(Hours)
11.) Groundwater Elevation
1 I. 1) Surveyed Well Elevation (MSL) _______ (feet) Data Not Available ___ _
I 1.2) Static Water Level Z 1 ;-,I (feet)
11.3) Static Water Elevation (MSL) ___ -_____ (feet) .
d :\rni$c•f nn \gmdwL wp
RBin
10 089
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Well m _ ___._..M_~ 1-,__9,____
12.) Well Sampling Data
12.1) Sample Collected
Test Parameters Bottle Type
''/t,(, \llrJ
Size
4b..,ij
2
Preservativo Number Collected
I+'(/) ti a
'
-
12.3) Sample Appearance: g Clear __ Sediment Toroid ---
12,4) Samples placed on ice immediately u\e,, collection:___;,_ Yes No
13.) Field Analyses
l'arameter
Tempera.lure ("Cl
pH
Conductivity
(uS/cm)
Types of pH Buffers Used:
d:\misc-frm\gmdwt.. wp
Calibration.Std.
NIA
4.C> f-,.D .
I i575r)
4.0
7.0
10.0
· Sample Reading
[(.,~
'?,'71
56
Lot Number ______ _
Lot Number -------1.otNumber ______ _
Std. After Sample
N/A
I ,Ob
qc,q
10 090
I
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Well ID __ ,_!{'-• JJ;_q~_
· 14.) Purge Summary
3/rt(qt; 3/q qs-Date & Time
1111t> 111'
Volume Purged L,Jf. 13 J/4 1;1 o;f I. rfoi
Well Tempc,raturc !?) (5,5 (~.5 (6.? r 6, 7
("C)
Well pH Rc.iding . 7\(3 5.q5 '5,72 ;71 5.11 ' ......_
Conductiv.\ty 77 (3 t I ,:6 7T
(uS/cm)
Other
Remarks
15.) Well secured with lock after sampling? -.!I,._ Yes No
16.) I, the undersigned, hereby certify that all of the above information is a=iratc.
NOTE: Certain information (such as well elevations and moan sea level heights of well casings) cannot bo
filled in on this form unless provided to IEA personnel by the client.
d :\misc-frm\g rndwt. wp
3
10 091
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NI 14uarion ec.,mpany
1.) Client Name:
2.) Client Location:
3.) Date:
4.) Well ID Number
6.) Sampler"s Name:
GROUNDWATER FIELD SAMPLING DATA SHEET
!EA, INC.
/.ke cJ,s f Cela(lt~t
SA(/16!/} NC
-2/q!__q,;
I ( 61,-53 5.)
CbQi.s Ovi:la,;)
Sampling Sequence #: 3 a
();;m 6M(Mi
1
7 .) Evacuatfon Method: ___ Bailer ___ Airlift Pump ___ Bladder Pump K . Other
8.) Sampling Method: ___ Bailer ___ Bladder Pump ___ ID Number
9.) Field Ob,:ervations and Sampling Conditions
9.1) Outside Temperature: J. C'C)
W cather Conditions: Clear _Js_Cloudy Calm __ W-mdy Rain
9.2) Was the well loclccd upon arrival? -¼. Yes No
9.3) An:1 unusual conditions in the an:a7 . __ Yes -fi.-NO
If •y cs• explain:
10.) ·well Evacuation (all =cots arc referenced from the top of the well casing)
10.1) Casing Diameter (ID): fl._ • {!1) (mches)
10.2) Total Well Depth: 6i ._@_ (feet)
10.3) Static Wattr Level: l O -~ (feet)
10.4) Height of Water Column: t/ 5 • 3 Q (fcet)(lQ.2.-.:: 10.3)
10.5) Water Volwno in Well: / • D 'f (liters/~
10.6) Eva,iiate 3 . l1I) Well Volu cs Prior to Sampling
10. 7) Evacuate ], 7, • O:V (Utersf~~!)Prior tci Sampling (10.6 • 10.S)
Timo Evacuation Started / 0 : · (Use 24 Hour Tune)
Time Evacuation Completed I! : O (Use 24 Hour Time}
10.8) Aclllctl Volume Evacuated ~ (Liters/~ .
10.9) Did the well go dry? __j._,_ Yes ,----No / ,,
A) Time well went dry _J!_: ~ I) Da~ ~~ lj >>
B) Time well was sampled IL . : r ( Date --_/ 9 s
C) Total time between evacuation and sampling ____ 3~S:~,m,,,,=· "'""'"'-------(Hours)
l 1.) Groundwater Elevation
11.1) Surveyed Well Elevation (MSL} _______ (feet) Data Not Available--=--=--
11.2) Static Water Level (Q ,10 (feet)
11.3) Static Water Elevation (MSL) -(feet) --------
d:\misc.frm\gmdwt,wp
10 092
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Well ID tl-5'J
12.) Well S.impling Data
12.1) Sample Collected
Test Panuneters Bottlo Typo
'I/JG v1cJ
2
Siz.e Preservative Number Collected
~o~ \t1,SD~ (j,
I 12.3) Sam.pie Appearance: '\. Oear ___ Sediment Turbid ---
12.4) Samples placed on ice immedia!cly afte,-collection: -1..-Yes No
I 13.) Field Analyses
I
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I
Parameter Calibration Std.
Temperature (°C) NIA
pH if.C> I, -D
' Conductivity
(uS/cm) 11257")
Types of pH Buffers Used: _-_ 4.0
7.0
10.0
I d:lmi,e•fnnlgmdwt.wp
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I
· Sample Reading
/', ,1
f,2'?
Lil
Lot Number ______ _
Lot Number -------Lot Number -------
.Std. After Sample
NIA
7.,(50
qqq
lQ 093
I Well ID _ ___,_N_,__-..:5:..>3'-----3
I ~4.) Purge Sumrn.uy
'. 1,.. J'
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Date & Time
Volume :?urged
Well Temiieroure
("Cl
Well pH Reading
Conductivity
(uS/cm)
Other
Rcm.trl<:s
)(1 q( -(( in'
L,it. 1
I~. 1-IS.1
i ,1) 'ii. I b
l.'.2-> -11·
/I~\ 3/qfa( 11 ~ . ~·· .
"1(
1¥ z1,/\l'\f L !£.
I "
I 5,7
i, '.2_)
•
i I
vJ
\I.J.O \If
I ·• , 15.) Well secured with lock aftei-ai:npling7 ~ Yes No
I
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16.) I, the undersigned, hereby certify that all of the above information is accurate.
Signature Date_~24-l°JLJ..lp..J..< __ _
NOTE: Certain information (such as well elevations and mean sea level heights of well casings) cannot bo
filled in ,on thil Cann nn1ess provided lo lEA pcrnonnel by tbe clienL
d:\mis.c-frm\gmdWLwp
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itf-\
M Aquarion Company
GROUNDWATER FIELD SAMPLING DATA SHEET
lEA, INC.
!.) Client Name:
2.) Client Location:
3.) Date: I I
4.) Well ID Number 0-2.6"
6.) Sampler's Name:
7.) Evacuatfon Method: Bailer ---___ . Airlift Pump ___ Bladder Pump
8.) Sampling Method: ___ Bailer ___ Bladder Pump ID Number ---
9.) Field Ob,:ervations and Sampling Conditions
;
9.1) Outside Temperature: ______ ("C)
l
_.,)(_~Other
Weather Conditions: Clear __ )(Cloudy __ Calm _Windy Rain
9.2) Was the well loeked upon arrival?
9.3) An)' unusual conditions in the a.re:,.?
---2!,_Yes
Yes
No
_LNo
If 'Yes' explain: ------------------------
10.) · Well Evacuation (all measurements arc referenced from the top of the well casing)
. 10.1)
10.2)
10.3)
10.4)
10.5)
10.6)
10.7)
Casing Diameter (ID): ,Q_ . 01> (Inches)
To~tl Well Depth: >--S • /Jb (feet)
Static Water Level: I? 75 (feet)
Height of Water Column: / • 1-~ (feet) i"~l0.3)
Wat,.r Volume in Well:-~-· 8 3 (liters/ . cins
Eva.c,uate __3_. pJ) Well -V~~ Prior to ling
Evacuate --1.R.._. m) (llters/[e-mail]) Prior to Sampling (10.6 • 10.S)
'D'me Evacuation Started ·I/ : t.f ( (Use 24 Hour Time)
lime Evacuation Completed I !.-: 05 (Use AHour Time)
10.8) Actu:tl Volume Evacuated /, • !fl} (llters/~) .
10.9) Did the well go dzy7 --~ Yes Y No
A) lime well went dry J)fo : Date
B) lime well was sampled / '2--.-:--Qz" Date ~~0~rq_f ___ _
C) Total time between evacuation and sampling ___________ (Hours)
11.) Groundwater Elevation
II.I) Surveyed Well Elevation (MSL) _______ (feet) Data Nol Available -
11.2) Static Watt:;r Level ! 3 ,JS (feet)
11.3) Static Watt:;r Elevation (MSL) ___ -_____ (feel)
d:\misc-frm\gmdwt.wp
10 095
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Well ID __ {)_-_]__~--
12.) Well Sampling Datn
12.1) Sample Collected
Test Parameters Bottle Typo
1DC VlrJl
2
Si.z.e Preservalivc Number Collected
1+aJ H/,b~ 8
I
I
I 12.3) Sample Appearance: ___ Clear ___ Sediment 'Y Turbid
12.4) Saraples placed on ic,, irnmrxliatcly after collection: ---2!.-Yes No
I 13.) Field Aaal yses
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Parameter
Temperature ("C)
pH
Conductivity
(uS/cm)
Types of pH Buffers Used:
d:\mi~•frm\gmdwt.wp
Calibration Std.
NIA
4.C> f 1 -D .
I /5l5r)
4.0
7.0
10.0
Sample Reading
/'i I'(
/, 114
~&Cf
Lot Number -------Lot Number -------Lot Number -------
Std. After Sample
NIA
1.ol>
q'n'
10 096
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l1
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Well ID -~Q'----.-'JS=----3
-, 4.) Purge Summary
3ftz -,/q/q{
Date & Time
.
/?-I)<;
Volume Purged LJt. 7 z/ i/',R. v H li1,
Well Temp<>rature ( s ,s I
I~,\ ,~. ~ I 3 ,4 8,2. (°C)
Well pH Reading 6,3/ t~o ~,45' 1.44 b,'-i~
Conductivity ~qJ 01S q~~ q6~ ~7t (uS/em)
Other
Remarks
, 15.) Well secured •.vith lock after sampling7 _2_ Yes No
16.) I, the undersigned, hereby certify that all of the above information is accurate.
Date__,J,,__.l..yi1l .... 9s,___ __ _
NOTE: Certain information (such as well elevations and mean sea level heights of well casings) cannot be
filled in on this form unless provided to IEA personnel by the clienL
d:\misc~fnn\gmdwt.wp
10 097
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□ NPDES □ DRINKING WATER □ RCRA □OTHER _______ _
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PH# 919-677-0090
FAX# [phone]
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3000 WESTON PKWY.
CARY, N.C. 27513
PH I 919-677-0090
FAX I 919-677-0427
--

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Page ____ of ___ _
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- - -
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------
-
IE A 3000 WESTON PKWY.
CARY, N.C. 27513
PH # 919-677-0090
An Aqualion Company FAX# [phone]
0 DRINKING WATER O AGRA O OTHER _______ _
-- - -mm 46577
Page ___ of __ _
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-------------·--CHAIN OF CUSTODY RECORD II I EA 3000 WESTON PKWY.
CARY, N.C. 27513
PH# 919-677-0090
An Aquarion Company FAX# [phone]
----
D NPDES □ DRINKING WATER D RCRA D OTHER ______ _
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Page ___ of __ _
l---+--1----1~-4--
- - -- - ----------CHAIN OF CUSTODY RECORD -111111 IEA ~ An Aquarion Company
3000 WESTON PKWY.
CARY, N.C. 27513
PH# 919-677-0090
FAX# [phone]
' ..
[] NPDES O DRINKING WATER [] RCRA [] OTHER _______ _
Page ___ of __ _
---__ L.>.._--\---~-....J--....J---l---J---J---1---1----·I----!--
, ___ 1------1-------1-----------1-'------------!--+---+---+---------------1----l--
0·<>.: REMARKS ON:SA
[J 130 lTLE lf-.l 1/1.C r [] CLJS I ODY SEALS
CJ PHESERVED JJ SEALS INTACT
I] CHILI.ED • I] SEE REMARKS
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Attachment 6
Analytical Data for the
March 6-9, 1995 Sampling Event
-------------------
SAMPLE ID
STEIN
STEIN
LAMBERT
LAMBERT
MARTIN
LABID
950319501
950319501
950319502
950319502
950319503
MARTIN 950319503
WALKER 950319504
WALKER 950319504
TRIP BLANK 03106195 950319505
C-49
FF-62
FF-34
OT EFFL
OT EFFL
OT EFFL
OT EFFL
ITEFFL
IT EFFL
IT EFFL
ITEFFL
IT EFFL
INTINFL
INT INFL
OTINFL
950319506
950319507
950319508
950319509
950319509
950319509
950319509
950319510
9503195 IO
950319510
950319510
950319510
950319511
950319511
950319512
TRIP BLANK 03107195 950319513
FP SLUDGE 950319714
FP SLUDGE
FP SLUDGE
FP SLUDGE
FP SLUDGE
EE-58
T-35
950319714
950319714
950319714
950319714
950320315
950320316
MASTER SAMPLE TRACKING LIST
DATE
SAMPLED
03106195
03106195
03106195
03106/95
03106195
03106195
03106195
03106195
03107195
03107195
03107195
03107195
03107195
03107195
03107195
03107195
03107195
03107195
03107195
03107195
03107195
03107195
03107195
03107195
03107195
03107195
03107195
03107195
03107195
03/08195
03108195
DATE ANALYSIS
RECEIVED TYPE PREP DATE
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03108195
03/08195
03108195
03108195
03108195
03108195
03108195
8240 VOA
INORGANICS
8240 VOA
INORGANICS
8240 VOA
INORGANICS
8240 VOA
INORGANICS
8240 VOA
8240 VOA
8240 VOA
8240 VOA
8240 VOA
8270 SEMIVOA
8080 PEST
INORGANICS
8240 VOA
8270 SEMIVOA
8080 PEST
03116195 , 03129195
03116195, 03/29195
03116195, 03129195
03116195, 03/29195
03112195
03113195
03116195 , 03129195
03112195
03113195
INORGANICS 03116195, 03129195
ETHYLENE GLYCOL NIA
8240 VOA
ETHYLENE GLYCOL NIA
8240 VOA
8240 VOA
TCLP PEST
TCLPVOA
TCLP SEMIVOA
TCLP HERB
03/17195
03/14195
03/16195
03120195
TCLP INORGANICS 03/16195, 03/29195
8240 VOA
8240 VOA
ANALYSIS DATE
03ii 7/95
03116195, 03130195
03/17195
03116195, 03130195
03117195
03116195, 03130195
03117195
03116195, 03130195
03117195
03118195
03/17195
03118195
03/18195
03118195
03122195
03116195, 03130195
03/18195
03/18195
03/22195
03116195, 03130195
03118195
03/18195
03/18195
03118195
03120195
03/23195
03127195
03123195
03/25195
03/16195, 03130195
03/20195
03/20195
...
0
0
---- -- -- -- - - -- -- -- -
MASTER SAMPLE TRACKING LIST N
0
DATE DATE ANALYSIS 0
SAMPLE ID LABID SAMPLED RECEIVED TYPE PREP DATE ANALYSIS DATE
HH-48 950320317 03/08/95 03/08/95 8240 VOA 03/2i/95
GG-61 950320318 03/08/95 03/08/95 8?.40 VOA 03/21/95
AA-54 950320319 n1.1no,,.,.,. ..,.,,vo/'::l:J 03/08/95 8240 VOA 03/21/95
V-23 950320320 03/08/95 03/08/95 8240 VOA 03/21/95
V-23 950320320 03/08/95 03/08/95 ETHYLENE GLYCOL NIA 03/18/95
ELLIOTT 95-0712 03/06/95 03/08/95 EPA 502.2 VOA 03/14/95 03/14195
ELLIOTT 95-0712 03/06/95 03/08/95 EPA 505 PEST 03/09/95 03/11/95
ELLIOTT 95-0712 03/06/95 03/08/95 EPA 525 SEMIVOA 03/11/95 03/11/95
STEIN 95-0712 03/06/95 03/08/95 EPA 502.2 VOA 03/14/95 03/14/95
STEIN 95-0712 03/06/95 03/08/95 EPA 505 PEST 03/09/95 03/11/95
STEIN 95-0712 03/06/95 03/08/95 EPA 525 SEMIVOA 03/11/95 03/11/95
LAMBERT 95-0712 03/06/95 03/08/95 EPA 502.2 VOA 03/14/95 03/14/95
LAMBERT 95-0712 03/06/95 03/08/95 EPA 505 PEST 03/09/95 03/11/95
LAMBERT 95-0712 03/06/95 03/08/95 EPA 525 SEMIVOA 03/11/95 03/11/95
MARTIN 95-0712 03/06/95 03/08/95 EPA 502.2 VOA 03/14/95 03/14/95
MARTIN 95-0712 03/06/95 03/08/95 EPA 505 PEST 03109195 03llli95
MARTIN 95-0712 03/06/95 03/08/95 EPA 525 SEMIVOA 03/11/95 03/11/95
WALKER 95-0712 03/06/95 03/08/95 EPA 502.2 VOA 03/14/95 03/14/95
WALKER 95-0712 03/06/95 03/08/95 EPA 505 PEST 03/09/95 03/11/95
WALKER 95-0712 03/06/95 03/08/95 EPA 525 SEMIVOA 03/11/95 03/11/95
TRIP BLANK 95-0712 03/06/95 03/08/95 EPA 502.2 VOA 03/14/95 03/14/95
-------------------
MASTER SAMPLE TRACKING LIST
SAMPLE ID LABID DATE SAMPLED DATE RECEIVED ANALYSIS PREP DATE DATE ANALYZED
--------
SBR Sludge 950320801 03/07/95 03/10/95 8240 VOA 03/19/95
SBR Sludge 950320801 03/07/95 03/10/95 TCLP 8270 VOA 03/16/95 03/23/95
SBR Sludge 950320801 03/07/95 03/10/95 8270 VOA 03/12/95 03/22/95
SBR Sludge 950320801 03/07/95 03/10/95 8080 PEST 03/13/95 03/24/95
SBR Sludge 950320801 03/07/95 03/10/95 TCLP 8080 PEST 03/17/95 03/23/95
SBR Sludge 950320801 03/07/95 03/10/95 TCLPHERB 03/20/95 03/25/95
SBR Sludge 950320801 03/07/95 03/10/95 METALS 03/21/95 03/15/95
SBR Sludge 950320801 03/07/95 03/10/95 TCLPMETALS 03/16/95 03/16/95
Trip Blank 3/5/95 950320802 03/05/95 03/10/95 8240 VOA 03/16/95
CC-33 950320803 03/09/95 03/10/95 8240 VOA 03/21/95
P-58 950320804 03109/95 03/10/95 8240 VOA 03/21/95
K-28 950320905 03/09/95 03/10/95 8240 VOA 03/21/95
Trip Blank 3/6/95 950320906 03/09/95 03/10/95 8240VOA 03/21/95
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I TCL-Volatiles (8240)
I Lambert
Walker
I Stein
Runyon
I IT lnf/Eff
OT lnf/Eff
I Monitor Wells
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11
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SDG NARRATIVE VOLATILE FRACTION
CASE: 619-690 SDG NO.: 03208 METHOD: SW-846 (8240)
SAMPLES: Six (6) Water Samples
This cast: was closed on March 10, 1995. These samples were received at Industrial and
Enviromnental Analysts, Inc. (IEA), each sample was assigned a 9-character "IEA" lab
identification number (lab ID) and a truncated client ID (for forms generation). This package
makes reforence to these !D's as listed on the IEA Assigned Number Index. AIi analyses were
performed according to approved methodologies and meet the requirements of the IEA Quality
Assurance Program. Please see the enclosed data package for your results and Chain of Custody
(COC) doc:umentation.
I certify that this data package is in compliance with the terms and conditions of the contract,
both technically and for completeness, for other than the conditions detailed above. Release of
the data contained in this hardcopy data package and on the computer-readable data on diskette
has been authorized by the laboratory manager or his designee, as verified by the following
signature.
03/24/95
Brian D. Neptune
Lead Analyst, GC/MS Final Review
IEA; Inc.
002
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lA CLIENT SAMPLE NC
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA Case No.: 619-687
Matrix: (soil/water) WATER
sample wt/vol:
Level: (low/med)
% Moisturi~: not dee.
5.0 (g/mL) mL
LOW
GC Column:DB-624 ID: 0.53 (mm)
LAMB
Method: 8240
SDG No.: 03195
Lab Sample ID: 950319502
Lab File ID: 0317K15.D
Date Received: 03/08/95
Date Analyzed: 03/17/95
Dilution Factor: 1.0
Soil Extract Volume: ___ (uL) Soil Aliquot Volume: __ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-1:17-3---------Chloromethane 10 u
74-83-9---------Bromomethane 10 u
75-01-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u
75-09-2---------Methylene chloride 5 u
67-64-1---------Acetone 10 u
75-15-0---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (total) 5 u
67-66-3---------Chloroform -5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-5_5·-6---------1, 1, 1-Trichloroethane 5 u
56-23-5---------Carbon Tetrachloride 5 u
7 5-2 7 ··4 ----:------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5------cis-1,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------trans-l,3-Dichloropropene 5 u
75-25-2---------Bromoform --5 u
108-10··1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane --5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
13 3 0-2 0··7-------Xylene (total) 5 u
FORM I VOA 3/90
012
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lA CLIENT SAMPLE Ni
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Nam,:: INDUSTRIAL & ENVIRONMENTA
Lab Codei: IEA Case No.: 619-687
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) mL
LOW
GC Columr,.:DB-624 ID: 0.53 (mm)
WALK
Method: 8240
SDG No.: 03195
Lab Sample ID: 950319504
Lab File ID: 0317914.D
Date Received: 03/-08/95
Date Analyzed: 03/17/95
Dilution Factor: 1.0
Soil Extract Volume: ___ (uL) Soil Aliquot Volume: __ (UL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
7 4-·8 7-3 ---'------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total) -67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
75-27-4---------Bromcidichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061·-02-6------trans-l, 3-Dichloropropene __
7 5-2 5··2---------Bromof orm
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane --108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41·-4--------Ethylbenzene
100-42··5--------styrene
1330-20-7-------Xylene (total)
FORM I VOA
10
10
10
10
5
10
5
5
5
5
5
5
10
5
5
5
5
5
2
5
5
5
5
5
10
10
5
5
5
5
5
5
5
u
u
u u u u u u u u u u u u u u u u
J u u u u u u u u u u u u u u
3/90
021
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lA CLIENT SAMPLE NC
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Namt,: INDUSTRIAL & ENVIRONMENTA
Lab Codes: IEA Case No.: 619-687
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) mL
LOW
GC Colwnn:DB-624 ID: 0.53 (mm)
STEIN
Method: 8240
SDG No.: 03195
Lab Sample ID: 950319501
Lab File ID: 0317904.D
Date Received: 03/08/95
Date Analyzed: 03/17/95
Dilution Factor: 1.0
soil Extract Volume: ____ (uL) Soil Aliquot Volume: ___ (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-93-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroeth~ne
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total) -67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
75-27-4---------Bromodichloromethane·
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-D1chloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
12 7 -18 ·· 4 --------Tetr achloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
13 3 0-2 0·-7-------Xylene (total)
FORM I VOA
Q
10 u
10 u
10 u
10 u
5 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
3/90
016
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lA CLIENT SAMPLE NC
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA Case No.: 619-687
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
5.0 (g/mL) mL
LOW
MART
Method: 8240
SDG No.: 03195
Lab Sample ID: 950319503
Lab File ID: 0317Kl6.D
Date Received: 03/08/95
Date Analyzed: 03/17/95
Dilution Factor: 1.0
% Moisture: not dee.
GC Column:DB-624
soil Extract Volume:
ID: 0.53 (mm)
___ (UL) Soil Aliquot Volume: ___ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 u
74-.33-9---------Bromomethane 10 u
75-01-4---------Vinyl Chloricte 10 u
75-00-3---------Chloroethane 10 u
75-09-2------~--Methylene Chloride 5 u
67-64-1---------Acetone 11
75-15-0---------carbon D1sulf1de 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-3----~----l,l-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (total) 5 u
67-66-3---------Chloroform -5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-55~6-~-------l,l,l-Trichloroethane 5 u
56-23-5---------Carbon Tetrachloride 5 u
7 5-2 7 ·-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5------cis-l,3-Dichloropropene 5 u
7 9-0 l-·6---------Tr ichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------trans-l,3-D1chloropropene 5 u
75-25-:,---------Bromoform --5 u
108-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7-------Xylene (total) 5 u
FORM I VOA 3/90
013
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lA CLIENT SAMPLE NO.
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA Case No.: 619-687
Matrix: (soil/water) WATER
Sample rt/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) mL
LOW
GC Column:DB-624 ID: 0.53 (mm)
C49
Method: 8240
SDG No.: 03195
Lab Sample ID: 950319506
Lab File ID: 0317J09.D
Date Received: 03/08/95
Date Analyzed: 03/18/95
Dilution Factor: 1.0
Soil Extract Volume: ____ (uL) Soil Aliquot Volume: __ (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
7 4-8 7 ·-3---------Chloromethane
74-83··9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-35--4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
54 0-59-·0--------1, 2-Dichloroethene (total) -67-66-:::---------Chlorofonn
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
·56-23~5---------carbon Tetrachloride
7 5-27-4 ··--------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01.-5------cis-1,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02··6------trans-1, 3-Dichloropropene
75-25-2--·-------Bromofonn --
108-10-1-·-------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--·------styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
10 u
10 u
10 u
10 u
5 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
5 u
,5 u.
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
1.0 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
3/90
1 o:::e
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lA CLIENT SAMPLE NC
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Nam,a: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA Case No.: 619-690
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) mL
LOW
GC Columr.i:DB-624 ID: 0.53 (mm)
K28
Method: 8240
SDG No.: 03208
Lab Sample ID: 950320905
Lab·File ID: 0321E09.D
Date Received: 03/10/95
Date Analyzed: 03/21/95
Dilution Factor: 1.0
Soil Extract Volume: ____ (uL) Soil Aliquot Volume: __ (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
7 4-·8 7-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-j'.5-0---------carbon Disulfide
75-::,5-4---------1, 1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)_
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-9:3-3---------2-Butanone
71-5!i-6---------l, i, 1-Trichloroethane
56-23-5---------Carbon-Tetrachloride-
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
12 4-4,8-1--------Dibromochloromethane
79-00·-5---------1, 1, 2-Trichloroethane
71-43··2---------Benzene
10061-02-6------trans-1,3-Dichloropropene
75-25-·2---------Bromoform --
108-10-1--~-----4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
7_9-34-.5---------1, 1, 2, 2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-4 l ··4--------Ethylbenzene
100-42-·5--------styrene
1330-20-7-------Xylene (total)
FORM I VOA
10
10
10
10
5
10
5
5
5
5
5
5
10 '5
5 ..
5
5
5
5
5
5
6
5
5
10
10
5
5
5
5
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5
Q-
u u u u u u u
u u
u u u u u u u u u
u u u
u
u u u u u u u u u u
3/90
004
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I
lA CLIENT SAMPLE NC
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Nam,:: INDUSTRIAL & ENVIRONMENTA
Lab Code!: IEA Case No.: 619-690
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) mL
LOW
GC Column:DB-624 ID: 0.53 (mm)
P58
Method: 8240
SDG No.: 03208
Lab Sample ID: 950320904
Lab File ID: 0321E08.D
Date Received: 03/10/95
Date Analyzed: 03/21/95
Dilution Factor: 1.0
Soil Extract Volume: ____ (uL) Soil Aliquot Volume: __ (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)_
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-5~>-6---------1, 1, 1-Tricfiloroethane
56-23-5---------carbOn Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-1,3-Dichloropropene
79-0l·-6---------Trichloroethene
124-413-1--------Dibromochloromethane
79-00··5---------1, 1, 2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-1,3-Dichloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
12 7 -18 ·-4 --------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88··3--------Toluene --
108-90··7--------Chlorobenzene
100-41-·4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
10 u
10 u
10 u
10 u
5 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
5 u
5 ·U
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
10 u
5 u
5 u
5 u
5 u
5 ·u
5 u
5 u
3/90
005
I
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I
I
I
I
I
I
I
I
I
I
,I
I
I
I
I
I
I
lA CLIENT SAMPLE NC
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Nam,;: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA Case No.: 619-687
Matrix: (soil/water) WATER
sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) mL
LOW
GC Column:DB-624 ID: 0.53 (mm)
T35
Method: 8240
SDG No.: 03195
Lab Sample ID: 950320316
Lab File ID: 0320E07.D
Date Received: 03/09/95
Date Analyzed: 03/20/95
Dilution Factor: 1.0
Soil Extract Volume: ___ (uL) Soil Aliquot Volume: __ (UL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q'
.
74-87-3---------Chloromethane 10 u
74-83-9---------Bromomethane 10 u
75-01-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u
75-09-2---------Methylene Chloride 5 u
67-64-1---------Acetone 10 u
75-15-0---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (total) 5 u -·67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 12
ll-55-6---------1,1,1-Trichloroethane 5 u
56-23-5--~-----~carbon Tetrachloride 5 u
75-27-4---------Bromodichloromethane 5 u
78-87-5-~-------l,2-Dichloropropane 5 u
10061 ·-01-5------cis-1, 3-Dichloropropene 5 u
79-01--6---------Tr ichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------trans-l,3-Dichloropropene 5 u
75-25-2---------Bromoform ·--5 u
108-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane --5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7-------Xylene (total) 5 u
FORM I VOA 3/90
017
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lA CLIENT SAMPLE NC
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA case No.: 619-687
Matrix: (soil/water) WATER
Sample 1o1t/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) mL
LOW
GC Column:DB-624 ID: 0.53 (mm)
V23
Method: 8240
SDG No.: 03195
Lab Sample ID: 950320320
Lab File ID: 0321K07.D
Date Received: 03/09/95
Date Analyzed: 03/21/95
Dilution Factor: 50.0
Soil Extract Volume: ____ (uL) Soil Aliquot Volume: __ (UL)
CA.5 NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
7 4-·8 7-3 __ .;. ______ Chloromethane
74-·83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2-~-------Methylene Chien.de
67-54-1---------Acetone
75-15-0---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene
67-66-3---------Chloroform
(total) -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
·56-23-5---------carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-1,3-Dichloropropene
79-01-6---------Trichloroethene
124-48~1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25--2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5--------~l,l,2,2-Tetrachloroethane --108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42··5--------styrene
1330-20-7-------Xylene (total)
FORM I VOA
500
500
500
500
250
500
250
250
250
250
250
250
500
250
250
250
250
250
250
250
250
250
250
250
500
500
250
250
250
250
250
250
250
Q
u u
u u
u
u u u u u u u u u u
u u u
u u u u u
u u u u u u u u u u
3/90
020
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lA CLIENT SAMPLE NO.
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA Case No.: 619-687
Matrix: (E;oil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) mL
LOW
GC Column:DB-624 ID: 0.53 (mm)
AA54
Method: 8240
SDG No.: 03195
Lab Sample ID: 950320319
Lab File ID: 0321K06.D
Date Received: 03/09/95
Date Analyzed: 03/21/95
Dilution Factor: 1.0
Soil Extrac:t Volume:
CAS .NO.
___ (uL)
COMPOUND
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
__ (uL)
Q
74-87-3---------Chloromethane 10 u
74-83-9---------Bromomethane 10 u
75-0l.-4---------vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u
75-09-2---------Methylene Chloride 5 u
67-64-1---------Acetone 10 u
75-15-0---------carbon Disulfide 5 u
75-35·-4---------1, 1-Dichloroethene 5 u
75-34·-3---------1, 1-Dichloroethane 5 u
·540-59-0--------1,2-Dichloroethene (total)_ 5 u
67-66··3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-23-5---------carbon.Tetrachloride 5 ,u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5------cis-1,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-·l--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------trans-l,3-Dichloropropene 5 u
75-25-2---------Bromoform --5 u
108-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5··--------l, 1, 2, 2-Tetrachloroethane --5 u
108-88-3:--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------Styrene 5 u
1330-20-7-------Xylene (total) 5 u
FORM I VOA 3/90
1
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lA CLIENT SAMPLE NC
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Cod,a: IEA Case No.: 619-690
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) mL
LOW
GC Column:DB-624 ID: 0.53 (mm)
CC33
Method: 8240
SDG No.: 03208
Lab Sample ID: 950320903
Lab File ID: 0321E07.D
Date Received: 03/10/95
Date Analyzed: 03/Z'!./95
Dilution Factor: 1.0
Soil Extract Volume: ____ (uL) Soil Aliquot Volume: __ (uL)
CONCENTRATION UNITS:
CJ\.S NO . COMPOUND (ug/L or ug/Kg) UG/L Q.
74-87-3---------Chloromethane 10 u
74-83-9---------Bromomethane 10 u
75-01-4---------Vinyl Chloriae 10 u
75-00-3---------Chloroethane 10 u
75-09-2---------Methylene Chloride 5 u
67-64-1---------Acetone 10 u
75-15-0---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (total)_ 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-:23-5---------carbon Tetrachloride 5 u
7 5-:! 7-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5------cis-1,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 14
10061-02-6------trans-1,3-Dichloropropene 5 u
75-2.5-2---------Bromoform --5 u
108-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-3~:-5---------1, 1, 2, 2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7-------Xylene (total) 5 u
FORM I VOA 3/90.
0-0 3
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lA CLIENT SAMPLE NO.
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code: :1n Case No.: 619-687
Matrix: (soil/water) WATER
EE58
Method: 8240
SDG No.: 03195
Lab Sample ID: 950320315
I Sample wt/vol: 5.0 (g/mL) mL
LOW
Lab File ID: 0320E06.D
Date Received: 03/09/95
Date Analyzed: 03/20/95
Dilution Factor: 1.0
I
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I
Level: (low/med)
% Moisture: not dee.
GC Column:DB-624 ID: 0.53 (mm)
Soil Extract: Volume: ____ (uL) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
7 4-83·-9---------Bromomethane
75-01··4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59·-0--------l, 2-Dichloroethene (total)_
67-66-3---------Chloroform
107-06·-2--------1, 2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1;1-Tricfiloroethane
56-23-5---------carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-1,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochlorometfiane
79-00-5··--------l, 1, 2-Trichloroethane
71-43-2··--------Benzene
10061-02:-6------trans-1, 3-Dicfiloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5----------1, 1, 2, 2-Tetrachloroetfiane __
108-88-3--------Toluene
108-9 0-7 ··-------Chlorobenzene
1 o 0-41-4 ··-------Ethy !benzene
100-42-5--------styrene
1330-20-7-------Xylene (total)
FORM I VOA
10
10
10
10
5
10
5
5
5
5
5
5
10
5
5
5
5
5
5
5
5
5
5
5
10
10
5
5
5
5
5
5
5
1
__ (uL)
Q
u u u u u u u u u u u u u . u u u u u u u u u u u u u u u u u u u u
3/90
041
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lA CLIENT SAMPLE NO.
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA Case No.: 619-687
Matrix: (so-il/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) mL
LOW
GC Column:OE:-624 ID: 0.53 (mm)
FF34
Method: 8240
SDG No.: 03195
Lab Sample ID: 950319508
Lab File ID: 0317J10.D
Date Received: 03/08/95
Date Analyzed: 03/18/95
Dilution Factor: 1.0
Soil Extract Volume: ____ (uL)
CAS NO . COMPOUND
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
__ (uL)
Q
.
74-87··3---------Chloromethane 10 u
74-83-·9---------Bromomethane 10 u
75-01-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u
75-09-2---------Methylene Chloride 5 u
67-64-1---------Acetone 10 u
75-15-0---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-:1---------1, 1-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (total)_ 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u
7 5-2 7 -4 ·---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5------cis-1,3-Dichloropropene 5 u
79-01-6··--------Trichloroethene 5 u
124-48-1.--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------trans-1,3-DJ.chloropropene 5 u
75-25-2---------Bromoform --5 u
108-10-1·--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4··-------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane 5 u
108-88-3--------Toluene --5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7-------Xylene (to£alj 5 u
FORM I VOA 3/90
1
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lA CLIENT SAMPLE NC
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA Case No.: 619-687
Matrix: (soil/water) WATER
sample wt/vol:
Level: (low/med)
% Moistur,~: not dee.
5.0 (g/mL) mL
LOW
GC Column::DB-624 ID: 0.53 (mm)
FF62
Method: 8240
SDG No.: 03195
Lab Sample ID: 950319507
Lab File ID: 0317J04.D
Soil Extra.ct Volume: ____ (uL)
Date Received: 03/08/95
Date Analyzed: 03/17/95
Dilution Factor: 1.0
Soil Aliquot Volume: __ (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloriae
75-00-3---------Chloroethane
75-09-2---------Methylene Chlon.de
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
7 9-0 l ··6---------Tr ichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-D1.chloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18··4--------Tetrachloroethene
79-34-5~--------l,l,2,2-Tetrachloroethane
108-88--3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (to'Ealj
FORM I VOA
Q
10 u
10 u
10 u
10 u
5 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
5 u
5 u
·5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
3/90
007
I
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lA CLIENT SAMPLE NC
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA case No.: 619-687
Matrix: (soil/water) WATER
GG61
Method: 8240
SDG No.: 03195
Lab Sample ID: 950320318
Sample wt/vol: 5.0 (g/mL) mL
LOW
Lab File ID: 0320E09.D
Level: (low/med)
% Moistur•=: not dee.
GC Column::DB-624 ID: 0.53 (mm)
Date Received: 03/09/95
Date Analyzed: 03/21/95
Dilution Factor: 1.0
Soil Extra,ct Volume: ____ (uL) Soil Aliquot Volume: ___ (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-137-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloriae
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-1,3-Dichloropropene
79-01··6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00--5---------1, 1, 2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-1,3-Dichloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
12 7-18--4--------Tetrachloroethene
79-34-5---------1,1,2,2-T~trachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Xylene (total)
'
FORM I VOA
Q
10 u
10 u
10 u
10 u
5 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
5 .. u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
10 u
5 u
5 u
5 u
5 u
5 .u
5 u
5 u
3/90
008
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lA CLIENT SAMPLE N(
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Namei: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA Case No.: 619-687
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) mL
LOW
GC Column:DB-624 ID: 0.53 (mm)
HH48
Method: 8240
SDG No.: 03195
Lab Sample ID: 950320317
Lab File ID: 0320E08.D
Date Received: 03/09/95
Date Analyzed: 03/21/95
Dilution Factor: 1.0
Soil Extract Volume: ___ (UL)
COMPOUND
Soil Aliquot Volume: __ (uL)
CAS NO.
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
7 4 ··8 7-3---------Chloromethane
7 4 -·8 3-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-54-1---------Acetone
75-15-0---------carbon D1sulf1de
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene
67-66-3---------Chloroform
(total) -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5------~--carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
7 9-0 l. -6---------Tr ichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-D1chloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-113-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
10
10
10
10
5
10
5
5
5
5
5
5
10
5
5
5
5
5
170
5
5
5
5
5
10
10
5
5
5
5
5
5
5
-Q
u u u u u u u u u u u u u u u u u u
0 u u u u u u u u u u u u u
3/90
009
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lA CLIENT SAMPLE NC
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name,: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA Case No.: 619-687
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) mL
LOW
GC Column:DB-624 ID: 0.53 (mm)
INTIN
Method: 8240
SDG No.: 03195
Lab Sample ID: 950319511
Lab File ID: 0317313.D
Date Received: 03/08/95
Date Analyzed: 03/18/95
Dilution Factor: 2.0
Soil Extract Volume: ___ {UL) Soil Aliquot Volum~: __ {UL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q-
7 4-·8 7-3---------Chloromethane 20 u
74-83-9---------Bromomethane 20 u
75-01-4---------Vinyl Chloride 20 u
75-00-3---------Chloroethane 20 u
75-09-2---------Methylene Chloride 10 u
67-64-1---------Acetone 220
75-15-0---------carbon Disulfide 17
75-35-4---------1,1-Dichloroethene 10 u
75-34-3---------1,1-Dichloroethane 10 u
540-59-0--------1,2-Dichloroethene (total) -10 u
67-66-3---------Chloroform 10 u
107-06-2--------1,2-Dichloroethane 10 u
78-93-3---------2-Butanone 36
71-55-6--------~l,l,l-Trichloroethane 10 0
56-23-5---------carbon Tetrachloride 10 u
75-27~4---------Bromodichloromethane 10 u
78-87-5---------1,2-Dichloropropane 10 u
10061-01-5------cis-l,3-Dichloropropene 10 u
79-01-6---------Trichloroethene 10 u
124-48-1--------Dibromochloromethane 10 u
79-00-5---------1,1,2-Trichloroethane 10 u
71-43-2---------Benzene 36
10061-02-6------trans-l,3-Dichloropropene 10 0
75-25-2---------Bromoform --10 u
108-10-1--------4-Methyl-2-Pentanone 20 u
591-78-6--------2-Hexanone 20 u
127-18-4--------Tetrachloroethene 10 u
7 9-3 4 ·-5---------1, 1, 2 , 2-Tetrachloroethane --10 u
108-88-3--------Toluene 10 u
108-90-7--------Chlorobenzene 17
100-41-4--------Ethylbenzene 10 u
100-42:-5--------styrene 10 u
1330-20-7-------Xylene (total) 10 u
FORM I VOA 3/90
010
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lA CLIENT SAMPLE NC
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name,: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA case No.: 619-687
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: · not dee.
5.0 (g/mL) mL
LOW
GC Column:DB-624 ID: 0.53 (mm)
ITEFF
Method: 8240
SDG No.: 03195
Lab Sample ID: 950319510
Lab File ID: 0317Jl2.D
Date Received: 03/08/95
Date Analyzed: 03/18/95
Dilution Factor: 1.0
Soil Extract Volume: ____ (UL) Soil Aliquot Volume: __ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q-
7 4-·8 7 -3 ---------Chloromethane 10 u
74-83-9---------Bromomethane 10 u
75-01-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u
75-09-2---------Methylene Chloride 5 u
67-64-1---------Acetone 10 u
75-15-0---------carbon Disulfide 5 u
75-J5-4---------l,l-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
54 0-·59-0--------1, 2-Dichloroethene (total) -5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-23-5---------Carbon Tetrachloride 5 u
75-27.:.4--------~Bromodichloromethane . 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5------cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------trans-l,3-Dichloropropene __ 5 u
75-25-2---------Bromoform 5 u
108-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-lH-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane 5 u
108-88-3--------Toluene --5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7-------Xylene (total) 5 u
FORM I VOA 3/90
011
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lA CLIENT SAMPLE NC
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA Case No.: 619-687
Matrix: (soil/water) WATER
sample wt/vol:
Level: (low/med)
5.0 (g/mL) mL
LOW
OTINF
Method: 8240
SDG No.: 03195
Lab Sample ID: 950319512
Lab File ID: 0317J14.D
Date Received: 03/08/95
Date Analyzed: 03/18/95
Dilution Factor: 1.0
% Moisture: not dee.
GC Colwnn:DB-624
Soil Extract Volume:
ID: 0.53 (mm)
___ (uL) Soil Aliquot Volume: ___ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 u
74-83-9---------Bromomethane 10 u
75-01-4---------Vinyl Chloriae 10 u
75-D0-3---------Chloroethane 10 u
75-09-2---------Methylene chloride 5 u
67-64-1---------Acetone 10 u
75-15-0---------carbon Disulfide 5 u
75-J5-4---------l,l-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-o--~-----l,2-Dichloroethene (total)_ 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56~23-5---------carbon Tetrachloride 5 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
1006:L-01-5------cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
12 4 -~; 8 -1--------D ibromochloromethane 5 u
79-0Cl-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------trans-l,3-Dichloropropene 5 u
75-25-2---------Bromoform --5 u
1os-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6~-------2-Hexanone 10 u
12 7 -1-9 -4 --------Tetrachl oroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7-------Xylene (total) 5 u
FORM I VOA 3/90
015
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lA CLIENT SAMPLE NC
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code.: IEA case No.: 619-687
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) mL
LOW
GC Column:DB-624 ID: 0.53 (nun)
OTEFF
Method: 8240
SDG No.: 03195
Lab Sample ID: 950319509
Lab File ID: 0317Jll.D
Date Received: 03/08/95
Date Analyzed: 03/18/95
Dilution Factor: 1.0
Soil Extract Volume: ____ (uL)
CAS NO. COMPOUND
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
__ (uL)
Q
74-87-3---------Chloromethane 10 u
74-33-9---------Bromomethane 10 u
75-01-4---------Vinyl Chloriae 10 · u
75-00-3---------Chloroethane 10 u
75-09-2---------Methylene Chlon.de 5 u
67-64-1---------Acetone 10 u
75-15-0---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (total) 5 u -67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1;1-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5· u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5------cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------trans-l,3-Dichloropropene 5 u
75-25·-2---------Bromoform --5 u
108-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4----:-----Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane --5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene ·5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------Styrene 5 u
1330-20-7-------Xylene (total) 5 u
FORM I VOA 3/90
014
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lA CLIENT SAMPLE NC
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA Case No.: 619-690
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) mL
LOW
GC Column:DB-624 ID: 0.53 (mm)
SBR
Method: 8240
SDG No.: 03208
Lab Sample ID: 950320801
Lab File ID: 0319J04.D
Date Received: 03/09/95
Date Analyzed: 03/19/95
Dilution Factor: 1.0
Soil Extract Volume: ____ (uL) Soil Aliquot Volume: __ (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-:33-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)_
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-5:i-6---------1, 1, 1-Trichloroethane
56-23-5---------carbon Tetrachloride
75-27-4---'------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-4S-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-·02-6------trans-1, 3-Dichloropropene __
75-25--2---------Bromoform
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42··5--------styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
10
10
10
10
5
10
5
5
5
5
5
5
10
5
5
5
5
5
5
5
5
5
5
5
10
10
5
5
5
5
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5
u u
u u u u u u u u u
u u u
u u u u u u u
u u
u
u u u u u u u u
u
3/90
006
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lA CLIENT SAMPLE N<
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Namei: INDUSTRIAL & ENVIRONMENTA
Lab Code,: IEA Case No.: 619-690
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
5.0 (g/mL) mL
LOW
TB35
Method: 8240
SDG No.: 03208
Lab Sample ID: 950320802
Lab File ID: 0316905.D
Date Received: 03/09/95
Date Analyzed: 03/16/95
Dilution Factor: 1.0
% Moistw:e: not dee.
GC Column:DB-624
Soil Extract Volume:
ID: 0.53 (mm)
____ (uL) Soil Aliquot Volume: __ (uL)
CONCENTRATION UNITS:
CA:5 NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10
74-·83-9---------Bromomethane 10
75-01-4---------Vinyl Chloride 10
75-00-3---------Chloroethane 10
75-09-2---------Methylene Chlon.de 5
67-64-1------~-~Acetone 10
75-15-o---------carbon D1.sulf1.de 5
75-35-4---------1,1-Dichloroethene 5
75-34-3---------1,1-Dichloroethane 5
540-59-0--------1,2-Dichloroethene (total) 5 -67-66-3---------Chloroform 5
107-06-2--------1,2-Dichloroethane 5
78-93-3--~------2-Butanone 10
71-55-6-----~---1,1,1-Trichloroethane 5
56-23~5---------carbon Tetrachloride 5
75-27-4---------Bromodichloromethane 5
78-87-5---------1,2-Dichloropropane 5
10061-01-5------cis-1,3-Dichloropropene 5
79-01-6---------Trichloroethene 5
124-48-1--------Dibromochloromethane 5
79-00-5---------1,1,2-Trichloroethane 5
71-43-2---------Benzene 5
10061-02-6------trans-1,3-D1.chloropropene 5
75-25-2---------Bromoform --5
108-10-1--------4-Methyl-2-Pentanone 10
591-78-6--------2-Hexanone 10
127-18-4--------Tetrachloroethene 5
79-34-5---------1,1,2,2-Tetrachloroethane --5
108-88-3--------Toluene 5
108-90-7--------Chlorobenzene 5
100-41-4--------Ethylbenzene 5
100-4 ,:-5--------Styrene 5
1330-20-7-------Xylene (total) 5
FORM I VOA
u u u u u u u u u
u u u u u
·U u u u u
u u u u u u u u u u u u u
u
3/90
007
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lA CLIENT SAMPLE Nt
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name,: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA Case No.: 619-690
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
5.0 (g/mL) mL
LOW
TB36
Method: 8240
SDG No.: 03208
Lab Sample ID: 950320906
Lab File ID: 0321El0.D
Date Received: 03/10/95
Date Analyzed: 03/21/95
Dilution Factor: 1.0
% Moisture: not dee.
GC Column:DB-624
Soil Extract Volume:
ID: 0.53 (mm)
___ (uL) Soil Aliquot Volume: ___ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10
74-83-9---------Bromomethane 10
75-01-4---------Vinyl Chloride 10
75-00-3---------Chloroethane 10
75-09-2---------Methylene Chloride 5
67-64-1---------Acetone 10
75-l.5-0---------carbon D1sulf1de 5
75-35-4---------1,1-Dichloroethene 5
75-34-3---------1,1-Dichloroethane 5
540-59-0--------1,2-Dichloroethene (total) 5 -67-66-3---------Chloroform 5
107-06-2--------1,2-Dichloroethane 5
78-93-3---------2-Butanone 10
71-~5-6---------1,1,1-Trichloroethane 5
56-2:l-5---------carbon Tetrachloride 5
75-27-4---------Bromodichloromethane 5
78-87-5---------1,2-Dichloropropane 5
10061-01-5------cis-l,3-Dichloropropene 5
79-01-6---------Trichloroethene 5
124-48-1--------Dibromochloromethane 5
79-00-5---------1,1,2-Trichloroethane 5
71-43··2---------Benzene 5
10061·-02-6------trans-l, 3-Dichloropropene 5
75-25··2---------Bromoform --5
108-10-1--------4-Methyl-2-Pentanone 10
591-78-6--------2-Hexanone 10
127-18-4--------Tetrachloroethene 5
79-34-5---------1,1,2,2-Tetrachloroethane 5
108-88-3--------Toluene --5
108-90-7--------Chlorobenzene 5
100-41-4--------Ethylbenzene 5
100-4 2 ·-5--------styrene 5
1330-20-7-------Xylene (total) 5
FORM I VOA
u u
u u u u
u u u
u u
u u u
u u
u u u u u
u u u u u u u u u
u u u
3/90
008
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lA CLIENT SAMPLE NC
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA Case No.: 619-687
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) mL
LOW
GC Column:DB-624 ID: 0.53 (mm)
TB36
Method: 8240
SDG No.: 03195
Lab Sample ID: 950319505
Lab File ID: 0317J03.D
Date Received: 03/08/95
Date Analyzed: 03/17/95
Soil Extr,3ct Volume: ___ (UL)
COMPOUND
Dilution Factor: 1.0
Soil Aliquot Volume: __ (UL)
CONCENTRATION UNITS:
CAS NO. (ug/L or ug/Kg) UG/L Q'
74-87-3---------Chloromethane 10 .U
74-83-9---------Bromomethane 10 u
75-01-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u
75-09-2---------Methylene Chloride 5 u
67-64-1---------Acetone 10 u
75-15-0---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (total) 5 u
67-66-3---------Chloroform -5 u·
107-06-2--------1,2-Dichloroethane 5 u
78-93-3-------~-2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride -5 u
75-27-4---------Bromodichloromethane -5 u
78~87-5---------1,2-Dichloropropane 5 u
10061-01-5------cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------trans-l,3-Dichloropropene 5 u
75-25·-2---------Bromoform --5 u
108-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane 5 u
108-88-3--------Toluene --5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7-------Xylene (total) 5 u
FORM I VOA 3/90
018
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lA CLIENT SAMPLE NC
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA case No.: 619-687
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) mL
LOW
GC Column:DB-624 ID: 0.53 (mm)
TB37
Method: 8240
SDG No.: 03195
Lab Sample ID: 950319513
Lab File ID: 0319J09.D
Date Received: 03/-08/95
Date Analyzed: 03/20/95
Dilution Factor: 1.0
Soil Extract Volume: ___ (UL)
COMPOUND
Soil Aliquot Volume: __ (uL)
CONCENTRATION UNITS:
CAS NO. (ug/L or ug/Kg) UG/L Q
74-.37-3---------Chloromethane
74-133-9---------Bromomethane
75~01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total) -67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
·75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-1,3-Dichloropropene
7 9-0 l·-6---------Trichloroethene
124-413-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-0ichloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---7-----1,1,2;2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-·5--------styrene
1330-20-7-------Xylene (total)
FORM I VOA
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3/90
019
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4A CLIENT SAMPLE NO.
SW-846 VOLATILE METHOD BLANK SUMMARY
Lab Nam,~: INDUSTRIAL & ENVIRONMENTA
Lab Codei: IEA Case No.: 619-690
Lab File ID: 0321E02.D
Date Analyzed: 03/21/95
GC Colum.n:DB-624
Instrument ID: MSD5
ID: 0.53 (mm)
VBLK51
Method: 8240
SDG No.: 03208
Lab Sample ID: VBLK51
Time Analyzed: 1842
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD
01
02
03
04
05
06
07
08
09
10
11
12
1:1
14,
l:; , 16
COMMENTS:
17
18
19
20
21
22
23
24
25
26
27
28
29
30
CJ.J.ENT
SAMPLE NO. ============
CC33
P58
K28
TB36
page 01 of 01
J..AB LAB 'l'J.ME
SAMPLE ID FILE ID ANALYZED --------------==---=========
950320903 0321E07.D 2154
950320904 0321E08.D 2232
950320905 0321E09.D 2309
950320906 0321El0.D 2345
FORM IV VOA 3/90
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4A CLIENT SAMPLE NO.
SW-846 VOLATILE METHOD BLANK SUMMARY
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA Case No.: 619-690
Lab File ID: 0316902.D
Date Analyzed: 03/16/95
GC Column:DB-624
Instrument ID: MSD9
ID: 0.53
VBLK93
Method: 8240
SDG No.: 03208
Lab Sample ID: VBLK93
Time Analyzed: 1004
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD
COMMENTS:
01
0 2
03
04
05
06
07
08
09
10
11
1·,
;
1:3
14
l:i
H
17
18
19
20
21
22
23
24
25
26
27
28
29
30
CLTENT
SAMPLE NO. ===--=====
TB35
page 01 of OJ.
LAB LAB TIME
SAMPLE ID FILE ID ANALYZED
=-==-====---= =====--======= --========
950320802 0316905.D 1319
FORM IV VOA 3/90
024
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lA CLIENT SAMPLE NC
SW-846 VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA case No.: 619-690
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.0 (g/mL) mL
LOW
GC Column:DB-624 ID: 0.53 (mm)
VBLK93
Method: 8240
SDG No.: 03208
Lab Sample ID: VBLK93
Lab File ID: 0316902.D
Date Received: / /
Date Analyzed: 03/16/95
Soil Extract Volume: ___ (UL)
COMPOUND
Dilution Factor: 1.0
Soil Aliquot Volume: __ (uL)
CONCENTRATION UNITS:
CA.S NO. (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane
74-.33-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene chloride
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)_
6 7-6,5-3 ---------Chlorof arm
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
7 5-2 7 -4------.---Bromodichloromethane
78-87-5--------~l,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-4:3-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,J-Dichloropropene
75-25-·2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane --108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-4 l ··4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Xylene (total)
FORM I VOA
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3/90
027
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IEA SDG NARRATIVE SEMIVOLATILE FRACTION
PROJECf: 619-690 BATCH: 03208 METHOD: SW-846 8270
Samples: (1) Water Sample
The samples were received at Industrial and Environmental Analysts, Inc. {IEA) on March 10, 1995.
The temperature upon receipt was 4°C. Each sample was assigned a 9-character "IEA" lab identification
number {lab ID) and an abbreviated client ID which is referenced on the IEA Assigned Number Index.
All analyses are performed in accordance with EPA approved methodologies and meet the requirements
of the IEA Quality Assurance Program. Please see the enclosed data package for your results and Chain
of Custody documentation.
The chrom1tographic separation of the analytes was performed using a Restek 30 X 0.32 XTI-5 fused
silica capillary column with a 0.5 µm bonded phase film thickness.
Instrument data printouts identify the compound 2,2 · -oxybis{ 1-Chloropropane) with CAS number 108-60-
1. Alternative nomenclature for this compound is bis(2-Chloroisopropyl)ether which is included on report
forms submitted.
The "J" flag indicates an estimated concentration below the quantitation limit and reported to 2.0 ng on
column.
The "M" flag used on the data system report form designates that a manual integration was required to
provide an accurate quantification of that analyte. · Manual integrations have been initialed and dated by
the analyst.
Samples SRB (950320801), SRBMS and .SRBMSD were initially analyzed at a dilution due to a high
concentration of non-target compounds present.
Matrix Spike/Matrix Spike Duplicate {MS/MSD) percent recovery for several compounds as noted on
the Form 3C exceed the limits specified for this method due to suspected matrix interference.
I certify that this data.package is in compliance with the procedures and methods defined for this project,
both teclmicaUy and for completeness, for other than the conditions detailed above. Release of the data
contained in this hardcopy data package and in the computer-readable data (if applicable) as submitted
has been authorized by the laboratory manager or his designee, as verified by the following signature.
µ t ,t.rr, ./\ . (1,1177. 03/28/95
Dawn A. Casto
GC/MS Data Reviewer
IEA, Inc.
1EA. Im: Docl RPF00701.NC
1
004
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1B CLIENT SAMPLE NC
SW-846 SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
OTEFF
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA case No.: 619-687 Method: 8270 SDG No.: 03195
Matrix: (soil/water) WATER Lab Sample ID: 950319509
Sample wt/vol: Lab File ID: 0317H06.D
Level: (low/med)
% Moisture:
500 (g/mL) mL
LOW
decanted: (Y/N)
Concentrated Extract Volume: 500 (UL)
Injection Volume: 2. 0 (UL)
Date Received: 03/08/95
Date Extracted:03/12/95
Date Analyzed: 03/18/95
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-~18-7---------2-Methylphenol
108-60-l--------bis(2-Chloroisopropyl)ether)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Iso~horone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol ·
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-B2-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-4 7 ·-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---~-----2,4,5-Trichlorophenol
91-58--7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
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10,
10,
10
50,
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u u
u u u u u
3/90
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lC CLIENT SAMPLE N•
SW-846 SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
OTEFF
Lab Nam,~: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA Case No.: 619-687 Method: 8270 SDG No.: 03195
Matrix: (soil/water) WATER Lab Sample ID: 950319509
Sample 1o1t/vol: Lab File ID: 0317H06.D
Level: (low/med)
% Moistu:re:
500 (g/mL) mL
LOW
decanted: (Y/N)
Concentrated Extract Volume: 500 (UL)
Injection Volume: 2.0(uL)
Date Received: 03/08/95
Date Extracted:03/12/95
Date Analyzed: 03/18/95
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100~01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-
101··55-3--------4-Bromophenyl-phenylether -
118··74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene ..
120-·12-7--------Anthracene
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-6B-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-5!5-3---------Benzo ( a) anthracene
21B-01-9--------Chrysene
117-Bl-7--------bis(2-Ethylhexyl)phthalate
117-E:4-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-B---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
Q
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u u u u u
u u
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100-51-6--------Benzyl Alcohol 20 'U
65-B5-0---------Benzoic Acid 50 u
FORM I SV-2 3/90
026
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lB CLIENT SAMPLE NC
SW-846 SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
ITEFF
Lab Name!: INDUSTRIAL & ENVIRONMENTA
Lab Codei: IEA Case No.: 619-687 Method: 8270 SDG No.: 03195
Matrix: (soil/water) WATER Lab Sample ID: 950319510
Sample wt/vol: Lab File ID: 0317H07.D
Level: (low/med)
% Moisture:
1000 (g/mL) mL
LOW
decanted: (Y/N) __
Concentrated Extract Volume: lOOO(uL)
Injection Volume: 2. 0 (uL)
Date Received: 03/08/95
Date Extracted:03/12/95
Date Analyzed: 03/18/95
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH:
CA.S NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-l--------bis(2-Chloroisopropyl)ether)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67 -· 7 2-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Iso~horone
88-75~5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dich~orophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-!i0-7---------4-Chloro-3-methylphenol
91-!i7-6---------2-Methylnaphthalene
77-4, 7-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
8 3-3 :2-9---------Acenaphthene
FORM I SV-1
Q
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u u u u u
3/90
023
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lC CLIENT SAMPLE NC
SW-846 SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
ITEFF
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Codei: IEA Case No.: 619-687 Method: 8270 SDG No.: 03195
Matrix: (soil/water) WATER Lab Sample ID: 950319510
Sample wt/vol: Lab File ID: 0317H07.D
Level: (low/med)
% Moisture:
1000 (g/mL) mL
LOW
decanted:
Concentrclted Extract Volume:
(Y/N)_
lOOO(uL)
Injection. Volume: 2.0(uL)
Date Received: 03/08/95
Date Extracted:03/12/95
Date Analyzed: 03/18/95
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5--7------2,4-Dinitrophenol
100~02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-
101··55-3--------4-Bromophenyl-phenylether -
118-74-1--------Hexachlorobenzene --
87-86~5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-Bl-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-3~3-5--------Indeno ( 1, 2, 3-cd) pyrene
53-70--3---------Dibenz (a, h) anthracene
191-24-2--------Benzo(g,h,i)perylene
100-51-6--------Benzyl Alcohol
65-85-0---------Benzoic Acid
FORM I SV-2
Q
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50
10
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10
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10
10
10
10
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3/90
024
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lB CLIENT SAMPLE N•
SW-846 SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SBR
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA case No.: 619-690 Method: 8270 SDG No.: 03208
Matrix: (soil/water) WATER Lab Sample ID: 950320801
Samplta wt/vol: Lab File ID: 0322411.D
Level: (low/med)
% Moisture:
500 (g/m.L) mL
LOW
decanted:
concentrated Extract Volume:
(Y/N)
500(uL)
Injection Volume: 2.0(uL)
Date Received: 03/09/95
Date Extracted:03/12/95
Date Analyzed: 03/22/95
Dilution Factor: 10.0
GPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-l--------bis(2-Chloroisopropyl)ether)
106·-4 4-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone ..
88-7.5-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
111-,11-1--------bis ( 2-Chloroethoxy) methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene•
106-47-8--------4-Chloroaniline
87-68-·3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-B--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
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100
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100
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u u
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u u u u u
u u
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u u
3/90
011
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lC CLIENT SAMPLE Nt
SW-846 SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SBR
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab C,:ide: IEA Case No.: 619-690 Method: 8270 SDG No.: 03208
Matrix: (soil/water) WATER Lab Sample ID: 950320801
Sample wt/vol: Lab File ID: 0322411.D
Level: (low/med)
% Moisture:
500 (g/mL) mL
LOW
decanted:
Concentrated Extract Volume:
(Y/N)
500(uL)
Injection Volume: 2. 0 (uL)
Date Received: 03/09/95
Date Extracted:03/12/95
Date Analyzed: 03/22/95
Dilution Factor: 10.0
GPC Cle2mup: (Y/N) N pH:
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-
101·-55-3--------4-Bromophenyl-phenylether -
118 -· 7 4-1--------Hexachlorobenz ene --
87~86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-8l-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--~~----Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-J---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
100-51-6--------Benzyl Alcohol
65-85-0---------Benzoic Acid
FORM I SV-2
Q
500
500
100
100
100
100
100
500
500
100
100
100
500
100
100
100
100
100
100
100
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100
100
100
100
100
100
200
500
u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u
3/90
012
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lD CLIENT SAMPLE NO.
SW-846 PESTICIDE ORG~.NICS ANALYSIS DATA SHEET
OTEFF
Lab Name: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA case No.: 619-687
Matrix: (soil/water) WATER
Method: 8080 SDG No.: 03195
Lab Sample ID: 950319509
Sample ';l',:/vol:
% Moisture:
500 (g/mL) ML
decanted: (Y/N)
Lab File ID: P6032295 008.D
Extracticm: ( SepF / Cont/ Sonc) SEPF
Concentrated Extract Volume: 5000(uL)
Injection Volume: 1. O (uL)
GPC Cleanup: (Y/N) N pH:
Date Received: 03/08/95
Date Extracted:03/13/95
Date Analyzed: 03/22/95
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) R
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
319-84-6--------alpha-BHC 0.030
319-85-7--------beta-BHC 0.050
319-86-8--------delta-BHC 0.050
58 ··8 9-9---------gamma-BHC (L1naanej 0.040
76-44-8---------Heptachlor 0.030
309-00-2--------Aldrin 0. 04 0
1024-57-3-------Heptachlor epox1ae 0.050
959-98-8--------Endosulfan I 0.050
60-57-1---------Dieldrin 0.046
72-55-9---------4,4'-DDE 0. 040
72-20-8---------Endrin 0.060
33213-65-9------Endosulfan II 0. 040
72-54-8---------4,4'-DDD 0.10
1031-07-8-------Endosulfan sulfate 0.10
50-29-3---------4,4'-DDT 0.10
72-43-5---------Methoxychlor 0.50
53494-70-5------Endrin ketone 0.10
7421-93-4-------Endrin aldehyeie 0.10
57-74-9---------Chlordane(technicalj 0.14
8001-35-2-------Toxaphene 5.0
12674-11-2------Aroclor-1016 0.50
11104-28-2------Aroclor-1221 0.50
11141-16-5------Aroclor-1232 0.50
53469-21-9------Aroclor-1242 0.50
12672-29-6------Aroclor-1248 0.50
11097-69-1------Aroclor-1254 1.0
11096-82-5------Aroclor-1260 1.0
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u u u u u u
u u u u u
u
FORM I PEST Rev 1. o 6/9·
031
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1D CLIENT SAMPLE NO.
SW-846 PESTICIDE ORGANICS ANALYSIS DATA SHEET
ITEFF
Lab Name: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA Case No.: 619-687
Matrix: (soil/water) WATER
Method: 8080 SDG No.: 03195
Lab Sample ID: 950319510
sample wt/vol:
% Moisture:
1000 (g/mL) ML
decanted: (Y /N)
Lab File ID: P6032295 006.D
Extraction: (SepF/Cont/Sonc) SEPF
Concentrc1ted Extract Volume: 10000 (UL)
Injection Volume: 1. 0 (UL)
GPC Cleanup: (Y/N) N pH:
Date Received: 03/08/95
Date Extracted:03/13/95
Date Analyzed: 03/22/95
Dilution Factor: l;0
Sulfur Cleanup: (Y/N) N
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
319-84-6--------alpha-BHC 0.030 u
319-85-7--------beta-BHC 0.050 u
319-86-8--------delta-BHC 0.050 u
58 ·-8 9-9---------gamma-BHC (Linoanej 0.040 u
76-44-8---------Heptachlor 0.030 u
309-00-2--------Aldrin 0.040 u
1024-57-3-------Heptachlor epoxioe 0.050 u
959-98-8--------Endosulfan I 0.050 u
60-57-1---------Dieldrin 0. 046 u
72-55-9---------4,4'-DDE 0.040 u
72-20-8---------Endrin 0.060 u
33213-65-9------Endosulfan II 0.040 u
72-54-8---------4,4'-DDD 0.10 u
1031-07-8-------Endosulfan sulfa'Ee 0.10 u
50-29-3---------4,4'-DDT 0.10 u
72-43-5---------Methoxychlor 0.50 u
53494-70-5------Endrin ketone 0.10 u
7421-93-4-------Endrin aldehyde 0.10 u
57-74-9---------Chlordane(technicalj 0.14 u
8001-35-2-------Toxaphene 5.0 u
12674-11-2------Aroclor-1016 a.so u
11104-28-2------Aroclor-1221 a.so u
11141-16-5------Aroclor-1232 a.so u
53469-21-9------Aroclor-1242 0.50 u
12672-29-6------Aroclor-1248 0.50 u
11097-69-1------Aroclor-1254 1.0 u
11096-82-5------Aroclor-1260 1.0 u
FORM I PEST Rev 1. 0 6/9·
029
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lD CLIENT SAMPLE NO.
SW-846 PESTICIDE ORGANICS ANALYSIS DATA SHEET
SBR
Lab Nam,~: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code,: IEA Case No.: 619-690
Matrix: (soil/water) WATER
Method: 8080 SDG No.: 03208
Lab Sample ID: 950320801
Sample wt/vol:
% Moistu:re:
1000 (g/mL) ML
decanted: (Y/N)_
Lab File ID: P6032295_034.D
Extracti<ln: (SepF /Cont/Sane) SEPF
concentrated Extract Volume: lOOOO(uL)
Injection Volume: 1. 0 (uL)
GPC Cleanup: (Y/N) N pH:
Date Received: 03/09/95
Date Extracted:03/13/95
Date Analyzed: 03/24/95
Dilution Factor: 10.0
Sulfur Cleanup: (Y/N) N
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
319-84-6--------alpha-BHC 0.30
319-85-7--------beta-BHC 0.50
319-86-8--------delta-BHC 0.50
58-89-9---------gamma-BHC (I:inaanej 0.40
76-44-8---------Heptachlor 0.30
309-00-2--------Aldrin 0.40
1024-57-3-------Heptachlor epoxiae 0.50
959-98-8--------Endosulfan I 0.50
60-57-1---------Dieldrin 0.46
72-55-9---------4,4'-DDE 0.40
72-20-8---------Endrin 0.60
33213-65-9------Endosulfan II 0.40
72-54-8---------4,4'-DDD 1.0
1031-07-8-------Endosulfan sulfate 1.0
50-29-3---------4,4'-DDT 1.0
72-43-5---------Methoxychlor 5.0
53494-70-5------Endrin ketone 1.0
7421-93-4-------Endrin aldehyde 1.0
57-74-9---------Chlordane(technicalj 1. 4
8001-35-2------~Toxaphene 50
12674--11-2------Aroclor-1016 5.0
11104-28-2------Aroclor-1221 5.0
11141-16-5------Aroclor-1232 5.0
53469-21-9------Aroclor-1242 5.0
12672-29-6------Aroclor-1248 5.0
.11097-69-1------Aroclor-1254 10
1109 6·-8 2 -5------Aroclor-12 6 O 10
u u
u u
u
u u
u u u
u u u u
u u
u u u u u
u u u u u u
FORM I PEST Rev 1.0 6/9
013
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4C
SW-846 PESTICIDE METHOD BLANK SUMMARY
Lab Name: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA Case No.: 619-690 Method: 8080
Lab File ID:
CLIENT SAMPLE NO.
PB550
SDG No.: 03208
P6032295 019.D Lab Sample ID: PB550
Matrix: (soil/water) WATER
Sulfur Cleanup: (Y/N) N
Date Analyzed (1): 03/23/95
Time Analyzed (1): 0958
Instrument ID (1): HP5890P6
Extraction: (SepF,Cont/Sonc) SEPF
Date Extracted: 03/13/95
GC Column (1) :RTX-35 ID: 0.53 (mm)
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD
COMMENTS:
page 01 of 01
01
02
03
04
05
06
07
08
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14
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18
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24
25
26
CLIENT
SAMPLE NO. =======;;;:====
SBR
SBRMS
SBRMSD
LCS550
LAB
SAMPLE ID
950320801
950320801MS
950320801MSD
LCS550
FORM IV PEST
DATE TIME
ANALYZED ANALYZED ========== ==========
03/24/95 1055
03/24/95 1209
03/24/95 1303
03/23/95 1122
3/90
035
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lD CLIENT SAMPLE NO.
SW-846 PESTICIDE ORGANICS ANALYSIS DATA SHEET
PB550
Lab Nam,:: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Cod,~: IEA Case No.: 619-690
Matrix: (soil/water) WATER
Method: 8080 SDG No.: 03208
Lab Sample ID: PB550
Sample .. t/vol:
% Moisture:
1000 (g/mL) ML
decanted: (Y /N)
Lab File ID:
Date Received:
P6032295 019.D
I I
Extraction: ( SepF / Cont/ sonc) SEPF
Concentrated Extract Volume: lOOOO(uL)
Injection Volume: 1. 0 (uL)
GPC Cleanup: (Y/N) N pH:
Date Extracted:03/13/95
Date Analyzed: 03/23/95
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
319-84-6--------alpha-BHC 0.030 u
319-85-7--------beta-BHC 0.050 u
319-86-8--------delta-BHC 0.050 u
58··89-9---------gamma-BHC (Linaanej 0.040 u
76-44-8---------Heptachlor 0.030 u
309-00-2--------Aldrin 0.040 u
1024-57-3-------Heptachlor epoxiae 0.050 u
959-98-8--------Endosulfan I 0.050 u
60-57-1---------Dieldrin 0. 046 u
72-55-9---------4,4'-DDE 0.040 u
72-20-8---------Endrin 0.060 u
33213-65-9------Endosulfan II 0.040 u
72-54-8---------4,4'-DDD 0.10 u
1031-07-8-------Endosulfan sulfate 0.10 u
50-29-3---------4,4'-DDT 0.10 u
72-43-5---------Methoxychlor 0.50 u
53494-70-5------Endrin ketone 0.10 u
7421-93-4-------Endrin aldehyde 0.10 u
57-74-9---------Chlordane(technicalj 0.14 u
8001-35-2-------Toxaphene 5.0 u
12674-11-2------Aroclor-lOlb 0.50 u
11104-28-2------Aroclor-1221 0.50 u
11141-16-5------Aroclor-1232 0.50 u
53469-21-9------Aroclor-1242 0.50 u
1267:2-29-6------Aroclor-1248 0.50 u
11097-69-1------Aroclor-1254 1.0 u
11096-82-5------Aroclor-1260 1.0 u
FORM I PEST Rev 1. O 6/9
036
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4C CLIENT SAMPLE NO.
SW-846 PESTICIDE METHOD BLANK SUMMARY
PB555
Lab Name: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Cod!:: IEA Case No.: 619-690 Method: 8080 SDG No.: 03208
Lab Sample ID: PB555
Matrix: (soil/water) WATER
Sulfur Cleanup: (Y/N) N
Date Analyzed (1): 03/22/95
Time Analyzed {1): 0638
Instrument ID (1): HP5890P4
Lab File ID: P4032195 019.D
Extraction: (SepF,Cont/Sonc) SEPF
Date Extracted: 03/17/95
GC Column (1) :DB-1701 ID: 0.53(mm)
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD
COMMENTS:
page 01 of 01
01
02
03
04
05
06
07
08
09
10
11
12
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17
18
19
20
21
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23
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25
26
CLIENT
SAMPLE NO.
--==========
SBR(TCLP)
TCLP239
SBRSPK
LAB
SAMPLE ID ==============
950320801{TCLP
TCLP239
950320801SPK
FORM IV PEST
DATE TIME
ANALYZED ANALYZED --------------------03/23/95 1537
03/22/95 1921
03/24/95 1643
3/90
037
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lD CLIENT SAMPLE NO.
SW-846 PESTICIDE ORGANICS ANALYSIS DATA SHEET
PB555
Lab Nam,~: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab CodE,: IEA Case No.: 619-690
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
% Moisture: ___ decanted: (Y/N)
Extraction: (SepF/Cont/Sonc) SEPF
Concentrated Extract Volume: lOOOO(uL)
Injection Volume: 1. 0 (uL)
GPC Cleanup: (Y/N) N pH:
Method: 8080 SDG No.: 03208
Lab Sample ID: PB555
Lab File ID: P4032195 Oi9.D
Date Received: / /
Date Extracted:03/17/95
Date Analyzed: 03/22/95
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N
CA,S NO. COMPOUND
CONCENTRATION UNITS:
(mg/Lor mg/Kg) MG/L Q
319-84-6--------alpha-BHC 0.000030 u
319-85-7--------beta-BHC 0.000050 u
319-86-8--------delta-BHC 0.000050 u
58-89-9---------gamma-BHC (L1.naanej 0.000040 u
76-44-8---------Heptachlor 0.000030 u
309-00-2--------Aldrin 0.000040 u
1024-57-3-------Heptachlor epox1.ae 0.000050 u
959-98-8--------Endosulfan I 0.000050 u
60-57-1---------Dieldrin 0.000046 u
72-55-9---------4,4'-DDE 0.000040 u
72-20-8---------Endrin 0.000060 u
72-54-8---------4,4'-DDD/Enao II 0.000040 u
1031-07-8-------Endosulfan sulfate 0.00010 u
50-29-3---------4,4'-DDT 0.00010 u
72-43-5---------Methoxychlor 0.00050 u
53494-70-5------Endrin ketone 0.00010 u
7421-93-4--~----Endrin aldehyae 0.00010 u
57-74-9---------Chlordane(technicalj 0.00014 u
8001-35-2-------Toxaphene 0.0050 u
12674-11-2------Aroclor-1016 0.00050 u
11104-28-2------Aroclor-1221 0.00050 u
11141-16-5------Aroclor-1232 0.00050 u
53469-21-9------Aroclor-1242 0.00050 u
12672-29-6------Aroclor-1248 0.00050 u
110517-69-1------Aroclor-1254 0.0010 u
11056-82-5------Aroclor-1260 0.0010 u
FORM I PEST 3/90
038
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lD CLIENT SAMPLE NO.
SW-846 PESTICIDE ORGANICS ANALYSIS DATA SHEET
PIBLKAA
Lab Name: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA case No.: 619-690 Method: 8080 SDG No.: 03208
I Matrix: (soil/water) WATER
Sample wt/vol: (g/mL)
Lab
Lab
Sample ID: PIBLKAA
File ID: P4032195 001.D
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% Moisture: ___ decanted: (Y/N) Date Received:
Extraction: (SepF/Cont/Sonc) Date Extracted:
concentr2,ted Extract Volume: ____ (uL) Date Analyzed: 03/21/95
Injection. Volume: 1. O (uL) Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: Sulfur Cleanup: (Y /N) N
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
319-84-6--------alpha-BHC 0.030 u
319-85-7--------beta-BHC 0.050 u
319-86-8--------delta-BHC 0.050 u
58··89-9---------gam.ma-BHC (Linclane) 0.040 u
76-44-8---------Heptachlor 0.030 u
309-00-2--------Aldrin 0.040 u
1024-57-3-------Heptachlor epoxicle 0.050 u
959-98-8--------Endosulfan I 0.050 u
60-57-1---------Dieldrin 0.046 u
72-55-9---------4,4'-DDE 0. 040 u
72-20-8---------Endrin 0.060 u
72-54-8---------4,4'-DDD/Eni:lo II 0.040 u
1031-07-8-------Endosulfan sulfate 0.10 u
50-29-3---------4,4'-DDT 0.10 u
72-43-5---------Methoxychlor 0.50 .u
53494-70-5------Endrin ketone 0.10 u
7421-93-4-------Endrin aldehyde 0.10 u
57-74-9---------Chlordane(technicalj 0.14 u
8001-35-2-------Toxaphene 5.0 u
12674-11-2------Aroclor-1016 0.50 u
11104-28-2------Aroclor-1221 0.50 u
11141-16-5------Aroclor-1232 0.50 u
53469-21-9------Aroclor-1242 0.50 u
12672-29-6------Aroclor-1248 0.50 u
11097-69-1------Aroclor-1254 1.0 u
11096-82-5------Aroclor-1260 1.0 u
FORM I PEST Rev 1. o 6/9'
040
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lD CLIENT SAMPLE NO.
SW-846 PESTICIDE ORGANICS ANALYSIS DATA SHEET
PIBLKFF
Lab Name: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA Case No.: 619-690 Method: 8080 SDG No.: 03208
Matrix: (soil/water) WATER
Sample wt/vol: (g/mL)
% Moisture: decanted: (Y/N)
Lab
Lab
Date
Sample ID: PIBLKFF
File ID: P6032295
Received:
001.D
I Extractic,n: (SepF /Cont/Sonc) Date Extracted:
Analyzed: 03/22/95
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concentrc,ted Extract Volume: ____ (uL) Date
Injection Volume: 1. 0 (UL) Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: Sulfur Cleanup: (Y/N) N
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
319-84-6--------alpha-BHC 0.030 u
319-85-7--------beta-BHC 0.050 u
319-86-8--------delta-BHC 0.050 u
5 8 ·-8 9-9---------gamma-BHC (:Cina:anej 0.040 u
76-44-8---------Heptachlor 0.030 u
309-00-2--------Aldrin 0.040 u
1024-57-3-------Heptachlor epoxia:e 0.050 u
959-98-8--------Endosulfan I 0.050 u
60-57-1---------Dieldrin 0.046 u
72-55-9---------4,4'-DDE 0.040 u
7 2-· 2 0-8---------Endr in 0.060 u
33213-65-9------Endosulfan II 0.040 u
72-54-8---------4,4'-DDD 0.10 u
1031-07-8-------Endosulfan sulface 0.10 u
50-29-3---------4,4'-DDT 0.10 u
72-43-5---------Methoxycblor 0.50 u
53494-70-5------Endrin ketone 0.10 u
7421-93-4-------Endrin aldehyae 0.10 u
57-74-9---------Chlordane(technicalj 0.14 u
8001-35-2-------Toxaphene 5.0 u
12674-11-2------Aroclor-1016 0.50 u
11104-28-2------Aroclor-1221 0.50 u
11141-16-5------Aroclor-1232 0.50 u
53469-21-9------Aroclor-1242 0.50 u
12672-29-6------Aroclor-1248 0.50 u
11097-69-1------Aroclor-1254 1.0 u
11096-82-5------Aroclor-1260 1.0 u
FORM I PEST Rev 1. o 6/9·
041
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lD CLIENT SAMPLE NO.
SW-846 PESTICIDE ORGANICS ANALYSIS DATA SHEET
PIBLKGG
Lab Name: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA case No.: 619-690 Method: 8080 SDG No.: 03208
Lab Sample ID: PIBLKGG Matrix: (soil/water) WATER
Sample wt/vol: (g/mL) Lab File ID: P6032295 016.D
% Moisture: decanted: (Y /N)
Extraction: (SepF/Cont/Sonc)
Concentrated Extract Volume:
Injection Volume: 1. 0 (uL)
GPC Clea:nup: (Y/N) N
____ (uL)
pH:
Date Received:
Date Extracted: ----
Date Analyzed: 03/23/95
Dilution Factor: 1.'0
Sulfur Cleanup: (Y/N) N
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q ,
319-84-6--------alpha-BHC 0.030 u
319-85-7--------beta-BHC 0.050 u
319-86-8--------delta-BHC 0.050 u
5E:-89-9---------gamma-BHC (Lina:anej 0.040 u
76-44-8---------Heptachlor 0.030 u
309-00-2--------Aldrin 0.040 u
1024-57-3-------Heptachlor epoxia:e 0.050 u
959-98-8--------Endosulfan I 0.050 u
60-57-1---------Dieldrin 0.046 u
72-55-9---------4,4'-DDE 0.040 u
72-20-8---------Endrin 0.060 u
33213-65-9------Endosulfan II 0.040 u
72-54-8---------4,4'-DDD 0.10 u
1031-07-8-------Endosulfan sulfate 0.10 u
50-29-3---------4,4'-DDT 0.10 u
7 2 ·-4 3-5---------Methoxychlor 0.50 u
53494-70-5------Endrin ketone 0.10 u
7421-93-4-------Endrin aldehya:e 0.10 u
57-74-9---------Chlordane(technical) 0.14 u
8001-35-2-------Toxaphene 5.0 u
12674-11-2------Aroclor-1016 0.50 u
lll.04-28-2------Aroclor-1221 0.50 u
11141-16-5------Aroclor-1232 0.50 u
53469-21-9------Aroclor-1242 0.50 u
12672-29-6------Aroclor-1248 0.50 u
11097-69-1------Aroclor-1254 1.0 u
11096-82-5------Aroclor-1260 1.0 u
FORM I PEST Rev 1. O 6/9-
042
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lD CLIENT SAMPLE NO.
SW-846 PESTICIDE ORGANICS ANALYSIS DATA SHEET
PIBLKHH
Lab Name,: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA Case No.: 619-690 Method: 8080 SDG No.: 03208
Matrix: (soil/water) WATER
sample wt/vol: (g/mL)
% Moisture: decanted: (Y/N)
Extracti,:m: ( SepF /Cont/ Sonc)
Concentrated Extract Volume:
Injection Volume: 1. 0 (uL)
___ (UL)
GPC Cleanup: (Y /N) N pH:
Lab Sample ID: PIBLKHH
Lab File ID: P6032295 -
Date Received:
Date Extracted:
Date Analyzed: 03/23/95
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N
Cl>.S NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
319-84-6--------alpha-BHC 0.030
319-85-7--------beta-BHC 0.050
319-86-8--------delta-BHC 0.009
58-89-9---------gamma-BHC (L1.naane) 0.040
76-44-8---------Heptachlor 0.030
309-00-2--------Aldrin 0.040
1024-57-3-------Heptachlor epoxiae 0.050
959-98-8--------Endosulfan I 0.050
60-57-1---------Dieldrin 0.046
72-55-9---------4,4'-DDE 0.040
72-20-8---------Endrin 0.060
33213-65-9------Endosulfan II 0.040
72-54-8---------4,4'-DDD 0.10
1031-07-8-------Endosulfan sulfa'Ee 0.10
50-29-3---------4,4'-DDT 0.10
7 2 ··4 3-5---------Methoxychlor 0.50
53494-70-5------Endrin ketone 0.10
7421-93-4-------Endrin aldehyae 0.10
57-74-9---------Chlordane(technical) 0.14
8001-35-2-------Toxaphene 5.0
12674-11-2------Aroclor-1016 0.50
11104-28-2------Aroclor-1221 0.50
11141-16-5------Aroclor-1232 0.50
53469-21-9------Aroclor-1242 0.50
12672-29-6------Aroclor-1248 0.50
11097-69-1------Aroclor-1254 1.0
11096-82-5------Aroclor-1260 1.0
032.D
u u
J u
u
u u u u
u u u u u
u u
u u u u u u u
u u u
u
FORM I PEST Rev 1. O 6/9-
043
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Chromium (601 Ol
Lambert
Walker
Stein
Runyon
Metals Analyses cs-zooo Series}
OT Eff
IT Eff
SBR W. Sludge
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IEA SDG NARRATIVE INORGANlC/IHETALS FRACTION
REVISED CASE NARRATIVE
CASE: 619 687 SDG NO.: 03195 CONTRACT: NIA
Samples: 9503 19502(LAMB); 9503 l 9503(MART); 950319501 (STEIN); and 9503 19504(W ALK) for
Chromium Analysis. 950319509(OTEFF); and 9503195 l0(ITEFF) for TAL Metals Analysis.
This case was closed on March 8, 1995. The temperature of the samples upon receipt by Industrial and
Environmental Analysts, Inc. (]EA) was 4°C. All samples were received intact.
The pH ol' sample ITEFF was seven (7) at the time of sample preparation.
The pH of all other samples for Metals analysis was less than two (2) at the time of sample preparation.
Each sample has been assigned a 9-character !EA lab identification number.
Any nonconformances associated with the analysis of samples in this case are noted as follows: The
original analysis of sample OTEFF for mercury gave a result of0.2177 ug/L. This sample was redigested
with batch 03169501 and reanalyzed with a result less than the instrument detection limit of 0.20 ug/L.
The latter result is being reported as it is in agreement with the duplicate and sample spike result.
I certify that this data package is in compliance with the terms· and conditions of the contract, both
technically and for completeness, for other than the conditions detailed above. Release of the data
contained in this hardcopy data package and in the computer-readable data submitted on diskette has been
authorized by the laboratory manager or his designee, as verified by the following signature.
norganic Data Reviewer
!EA, Inc.
!EA, Inc Doc# RPF00900.NC
1
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,I
IEA SDG NARRATIVE INORGA.t"IIC/METALS FRACTION
REVISED CASE NARRATIVE
CASE: 619 690 SDG NO.: 03208 CONTRACT: NIA
Sample: 950320801 (SBR) for TAL Metals Analysis
This case was closed on March 9, 1995. The temperature of the samples upon receipt by Industrial and
Environmental Analysts, Inc. (!EA) was 3"C. All samples were received intact.
This project was divided into two separate reports due to the different reporting limits for the leachates
and software limitations.
The pH of sample SBR was seven (7) at the time of sample preparation.
Each sample has been assigned a 9-character !EA lab identification number.
The "E" flag is used on Form 1 to identify a value that is estimated due to the presence of an
interferenc,:. For this sample, the "E" flags are due to high,conentrations of iron and manganese.
The"*" flag is used to identify a sample whose duplicate analysis exceeds the 20% RPO criteria. Sample
SBR is flagged with a "*" for chromium and lead.
The "N" flag is applied to any samples that do not meet acceptable spike recovery control limits of 75
to 125 % . Sample SBR is flagged with a "N" for thallium.
Sample SBR was diluted I OOX for mercury analysis due to excess foaming of the sample when analysis
was attempted.undiluted.
Sample SBR was redigested for metals analysis on batch 0321950 I due to an inconsistency between the
appearance of the sample and the duplicate and sample spike.
I certify that this data package is in compliance with the terms. and conditions of the contract, both
technically and for completeness, for other than the conditions detailed above. Release of the data
contained in lhis hardcopy data package and-in the computer-readable data submitted on diskette has been
authorized by the laboratory manager or his designee, as verified by the following signature.
Inorganic Data Reviewer
!EA, Inc.
[EA, Inc Doc# RPF00900.NC
1
U.S. EPA -CLP
1 EPA SAMPLE NO.
I
I INORGANIC ANALYSES DATA SHEET
I Lab
Lab
Name: INDUSTRIAL_AND_ENVIRONMEN
Code: IEA Case No:619-687
I Matrix (soil/water): .WATER
Level (low/med): LOW
I% Solids: 0.0
Contract:
SAS No.:
LAMB
SDG No.: 03195
Lab Sample ID: 950319502
Date Received: 03/08/95
I
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I
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8·
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I color Before: COLORLESS
Color After:
I Comments:
I
I
I
COLORLESS
Analyte Concentration C
-Aluminum
Antimony-· --Arsenic --Barium -Beryllium -Cadmium
Calcium--
Chromiwn 1.6 -B
Cobalt -Copper_ -Iron -Lead -Magnesium -Manganese -Mercury_ -Nickel -Potassium -Selenium -Silver
Sodium--
Thalliwn -
Vanadium= --Zinc -Cyanide_ --
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-NR
NR
NR
NR
NR
NR
NR
p -NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
-
Texture:
Artifacts:
3/90
036
·•
I
U.S. EPA -CLP
1
INORGANIC ANALYSES DATA SHEET
, b Name: INDUSTRIAL_AND_ENVIRONMEN Contract:
EPA SAMPLE NO.
WALK
f-Lab Code: I.EA__ Case No:619-687 SAS No.:
I Matrix (soil/water): WATER
.Level (low/med):
% Solids:
LOW
0.0
SDG No.: 03195
Lab Sample ID: 950319504
Date Received: 03/08/95
Concentration Units (ug/L or mg/kg dry weight): UG/L_
I
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I Color Before::
1 Color After:
Comments:
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte Concentration C
-Aluminum -Antimony_ -Arsenic --Barium -Beryllium -Cadmium
Calcium--
Chromium 1.0 u
Cobalt -Copper_ -Iron -Lead -Magnesium -Manganese -Mercury_ -Nickel -Potassium -Selenium -Silver
Sodium--
--Thallium
Vanadium---Zinc -Cyanide_ -
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-NR
NR
NR
NR
NR
NR
NR
p -NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
-
Texture:
Artifacts:
3/90
040
U.S. EPA -CLP
1 EPA SAMPLE NO.
I
I INORGANIC ANALYSES DATA SHEET
STEIN I Lab
Lab
Name: HlDUSTRIAL AND_ ENVIRONMEN Contract:
Code: IgA Case No:619-687 SAS No. : SDG No.: 03195_
Lab Sample ID: 950319501
Date Received: 03/08/95
I Matrix ( soiJ./water) : WATER
1 Level (low/med):
% Solids:
LOW
0.0
I
I
I
I
I
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Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I color Before: COLORLESS
I Color After:
Comments:
I
I
I
COLORLESS
Analyte Concentration C
-Aluminum
Antimony--
-Arsenic --Barium -Beryllium -Cadmium
Calcium--
Chromium 3.0 -B
Cobalt --Copper_· -Iron -Lead -Magnesium -Manganese -Mercury_ -Nickel -Potassium -Selenium -Silver
Sodium--
Thalliwn -
Vanadium= --Zinc -Cyanide_ -
--
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-NR
NR
NR
NR
NR
NR
NR
p
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
-
Texture:
Artifacts:
3/90
039
U.S. EPA -CLP
1 EPA SAMPLE NO.
I
I INORGANIC ANALYSES DATA SHEET
.Lab
Lab
Name: INDUSTRIAL_AND_ENVIRONMEN
Code: Il~A Case No:619-687
I Matrix ( soil./water) : WATER
Level (low/med):
1% Solids:
LOW
0.0
Contract:
SAS No.:
MART
SDG No.: 03195
Lab Sample ID: 950319503
Date Received: 03/08/95
I
I
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I
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No,
7429-'90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I Color Before: COLORLESS
Color After:
I comments:
I
I
I
COLORLESS
Analyte Concentration C
-Aluminum
Antimony--
Arsenic ----Barium -Beryllium -Cadmium
Calcium--
Chromium 5.5 -B -Cobalt -Copper_ -Iron -Lead -Magnesium -Manganese -Mercury_ -Nickel -Potassium -Selenium -Silver
Sodium--
Thalliwn -
Vanadium---Zinc -Cyanide -
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-NR
NR
NR
NR
NR
NR
NR
p
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
-
Texture:
Artifacts:
3/90
037
U.S. EPA -CLP
1 EPA SAMPLE NO. I
I INORGANIC ANALYSES DATA SHEET
.Lab
Lab
Name: INDUSTRIAL AND ENVIRONMEN
Code: IEA __
I Matrix (soil/water) :
Level (low/med) :
I% Solids:
Case No:619-690
WATER
LOW
0.0
Contract:
SAS No.:
SBR
SDG No,: 03208
Lab Sample ID: 950320801
Date Received: 03/09/95
I
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I
I
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I
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
.Color Before: BROWN
Color After: YELLOW
I Comments:
I
I
I
Analyte Concentration C Q
Aluminum 762 B
Antimony-32.8 B
Arsenic -30.0 u -Barium 10300 -Beryllium 10.0 u
Cadmium 28.2 B
Calcium-221000 E
Chromium 73.8 ---B * ---Cobalt 6130 E ---Copper_ 13.8 B
Iron 1090000 _E_
Lead 22.8 B *
Magnesium 174000 -E---E-Manganese 1630000
Mercury_ 20.0 u -N----Nickel 1760 -Potassium 110000 -Selenium 30.0 u
Silver 18.0 B
Sodium-575000 E
Thallium· 150 u -N-
Vanadium-10.0 ---u
Zinc 447 -Cyanide --
Clarity Before: CLOUDY
Clarity After: CLEAR
FORM I -IN
M
-p -p -p -p -p -p -p -p -p -p -p -p -p -p
CV
p -p -p -p -p -p -p -p -NR
-
Texture:
Artifacts:
3/90
4
I U.S. EPA -CLP
COVER PAGE -INORGANIC ANALYSES DATA PACKAGE
.Lab Name: INDUSTRIAL_AND_ENVIRONMEN Contract:
Code: IEA
No. : ILM03
Case No.:619-690 __ SAS No.: SDG No.:03208
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Were
lwere
EPA Sample No.
SBR --SBRM_S __ _
SBRMSD
==TB#239==
Lab Sample ID
950320801
-950320801MS
-950320801MSD
_TB#239 __ _
ICP inte,relement corrections applied ?
ICP background corrections applied?
If yes -were raw data generated before I application of background corrections?
Yes/No YES
Yes/No YES
Yes/No NO
Comments:
1 _____ tJ_a_o_bv_;_a<cli __ e_:,.p1_i::_,n_,;>=_e1-_:0_11_k __ i=_-_iv:._%_o_n_&_r_i""_,..._ ____________ _
Ir certify that this data package is in compliance with the terms and
conditions of the contract, both technically and for completeness, for
l ather than the conditions detailed above. Release of the data contained
in this hardcopy data package and in the computer-readable data submitted
on floppy disk,ette has been authorized by the Laboratory Manager or the
Manager's desiqnee, as verified by the following signature.
lsignature: _ 1/an,<'-< E, /'J'Ur{;_ k Name: Donald C. Stogner ___ _
j -1L2ib's-Title: Manager, Inorganics ---(I COVER PAGE -IN 3/90
I
I 4 395
U.S. EPA -CLP
1 EPA SAMPLE NO.
I
I INORGANIC ANALYSES DATA SHEET
I Lab Name: INDUSTRIAL AND ENVIRONMEN Contract:
Lab Code: IEA Case No:619-690 __ SAS No.:
I Matrix (soil/water): WATER
1 Level (low/med):
% Solids:
LOW
0.0
SER
SDG No.: 03208
Lab Sample ID: 950320801
Date Received: 03/09/95
I
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I
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I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
I Color Before:
.Color After:
Comments:
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
PINK __ _
YELLOW
Analyte Concentration C
-Aluminum
Antimony= --Arsenic 21. 0 u -Barium 306 B
Beryllium
Cadmium 3.0 u
Calcium-
Chromium 4.0 -u
Cobalt -Copper_ -Iron
Lead 21.0 u
Magnesium -Manganese -Mercury_ 20.0 u
Nickel -Potassium
Selenium 41.0 u
Silver 4.0 u
Sodium--Thallium
Vanadium---Zinc -Cyanide_ -
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q
E --
N --
M
NR
NR
p -p -NR
p -NR
p
NR
NR
NR
p -NR
NR
CV
NR
NR
p -p
NR
NR
NR
NR
NR
-
Texture:
Artifacts:
3/90
4 396 021
U.S. EPA -CLP
1 EPA SAMPLE NO.
I
I INORGANIC ANALYSES DATA SHEET
.Lab
Lab
Name: INDUSTRIAL_AND_ENVIRONMEN
Code: IEA Case No:619-687
I Matrix (soil/water) : WATER
Level (low/med):
I% Solids:
LOW
0.0
Contract:
SAS No.:
OTEFF
SDG No.: 03195
Lab Sample ID: 950319509
Date Received: 03/08/95
I
I
I
I
I
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I Color Before: YELLOW
Color After:
I comments:
I
I
I
COLORLESS
Analyte Concentration C
-Aluminum 32.5 B
Antimony-2.0 u
Arsenic -3.0 u -Barium 144 B
Beryllium 1. 0 u
Cadmium 1. 0 u
Calcium-19000
Chromium 1. 0 -u
Cobalt 4.7 B
Copper_ 1.0 u
Iron 621 -Lead 1.0 u
Magnesium 6940 -Manganese 317
Mercury_ 0.20 u
Nickel 1.0 u
Potassium 6770
Selenium 3.0 u
Silver 1.0 u
Sodium-50100
Thalliwn 3.0 -u
Vanadium-1.0 u
Zinc 34.8 -Cyanide_ --
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p -p -p -p -p -p -p -p -p -p -p -p -p -p
CV
p -p -p -p -p -p -p -p -NR
-
Texture:
Artifacts:
3/90
038
U.S. EPA -CLP
1 EPA SAMPLE NO.
I
I INORGANIC ANALYSES DATA SHEET
.Lab Name: INDUSTRIAL AND_ENVIRONMEN
Lab Code: IEA
.Matrix (soil/water):
Level (low/med) :
I% Solids:
Case No:619-687
WATER
LOW
0.0
Contract:
SAS No. :
ITEFF
SDG No.: 03195
Lab Sample ID: 950319510
Date Received: 03/08/95
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Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I Color Before: COLORLESS
Color After:
I comments:
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COLORLESS
Analyte Concentration C
-Aluminum 129 B
Antimony= 2.0 u
Arsenic 3.0 u -Barium 12.3 B
Beryllium 1.0 u
Cadmium 1. 0 u
Calcium-5720
Chromium 1.2 -B
Cobalt 36.5 B
Copper_ 2.4 B
Iron 1090 -Lead 1.0 u
Magnesium 27800 -Manganese 2310 -Mercury_ 0.20 u
Nickel 7.6 B
Potassium 3110 B
Selenium 3.0 u
Silver 1.0 u
Sodium-523000
Thal.limn 3.0 -u
Vanadium-1.0 u
Zinc 15.5 B
Cyanide_ -
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p -p -p -p -p -p -p -p -p -p -p -p -p -p
CV
p -p -p -p -p -p -p -p
NR
-
Texture:
Artifacts:
3/90
035
U.S. EPA -CLP
1 EPA SAMPLE NO. I
I
INORGANIC ANALYSES DATA SHEET
Lab Name: INDUSTRIAL_AND_ENVIRONMEN
ILab Code: I:E:A
.Matrix (soil/water):
Level (low/med) :
1% Solids:
Case No:619-690
WATER
LOW
0.0
Contract:
SAS No.:
TB#239
SDG No.: 03208
Lab Sample ID: TB#239
Date Received: 03/09/95
Concentration Units (ug/L or mg/kg dry weight): UG/L_
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1 Color Before:
Color After:
I Conunents:
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CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte Concentration C
-Aluminum
Antimony--
-Arsenic 21. 0 u -Barium 4.5 B
Beryllium
Cadmium 3.0 u
Calcium-
Chromium 4.0 -u
Cobalt --Copper_ -Iron -Lead 43.9 B
Magnesium -Manganese -Mercury_ 0.20 u
Nickel -Potassium -Selenium 41.0 u -Silver 4.0 u
Sodium--
Thalliiiin -
Vanadium--
--Zinc -Cyanide_ --
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q
E --
N ---
M
-NR
NR
p -p -NR
p
NR
p -NR
NR
NR
p
NR
NR
CV
NR
NR
p -p
NR
NR
NR
NR
NR
-
Texture:
Artifacts:
3/90
022
4 397
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Drinking Water Analyses
Volatiles /502.2), Semivolatiles /525}, Pesticides/PCBs /505}
Lambert
Walker
Stein
Runyon
Elliott
N0.444 P\2102
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II !§t~~
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,1 I l
CASE NARRATIVE (95-0712)
Re: Celane conference call.
An attempt at ~ calibration curve was made for method 502.2. The ¾RSDs ranged from 9-80%
v.ith the majo9ty falling between 30-50% RSD. In ac<:ordance with the method. a single point
calibration the' became a viable option. Everything was quantitated from the single point.
In regard to thj detection of 1,2-dichloroethane and benzene in the Martin sample, they are
correctly identfied as in the package.
1
Brian Cc,rbin 1·
QA Manager
6/8/95
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1A SAMPLE NO.
502.2 ANALYSIS DATA SHEET
Lab Name: IEA-FL ---------------
Proj1!Ct No.: ..:9c:5:..·.:.0.;.7.;.1 .:.2 _____ _
Matrix: (soil/water)
Level: (low/med)
Dill.ftion Factor:
CAS No.
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
WATER
LOW
1.0
Compound
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butyl benzene
tert-Butylbenzene
Carbon tetrachloride
Chiaro benzene
Chloroethane
Chloroform
· Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Oibromochloromethane
1,2-Dibromo-3-chloroorooane
1,2-Dibromoethane
Oibromomethane
1,2-Dichlorobenzene
1,3-0ichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifluoromethane
1, 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
cis-1,2-Dichtoroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
1,3-Dichloropropane
2 ,2-Dichloropropane
1, 1-Dichloropropene
cis-1 ,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
lsopropylbenzene
4-lsopropyltoluene
Methylene chloride
Naphthalene
Propylbenzene
Styrene
1, 1, 1,2-Tetrachloroethane
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2.3-Trichlorobenzene
1,2,4-Trichlorobenzene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
T richlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trfmethylbenzene
1 ,3,5-Trimethylbenzene
Vinyl chloride
Total Xvlenes
ELLIOT
Lab Sample ID: ..:E::L::L:.:10:..Tc_ __ _
Lab Fi!e 10: 712E ------
Date Sampled: 3/6/95 ------
Date Analyzed: 3/14/95 ------
Concentration Units:
{ug/L or ug/Kg) ug/1 Q
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0:50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
a.so u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u 051
1A SAMPLE NO.
I 502.2 ANALYSIS DATA SHEET
Lab Name: IEA-FL ..:.--------------STEIN
I Project No.: ..:9:.::5:...-0:.7:...1:..:2:_ ____ _
Matrix: (soil/water) WATER
Lab Sample ID: ..:S:...T..:E:...IN.;_ __ _
Lab File ID: ..:7..;1..:2..:S'----
LOW Date Sampled: ..:3c./6;c;/..:9..:5 ___ _
I Dilu·tion Fact:or: 1.0 Date Analyzed: ..:3;;.l.;.14-'l..:9..:5 __ _
Concentration Units:
I CAS No Compound (ug/L or ug/Kg) ug/I Q
71-43-2 Benzene 0.50 u
108-86-1 Bromobenzene 0.50 u
74-97-5 Bromochloromethane 0.50 u
I 75-27-4 Bromodichloromethane 0.50 u
75-25-2 Bromoform 0.50 u
74-83-9 Bromomethane 0.50 u
I 104-51-8 n-Buty!benzene 0.50 u
135-98-8 sec-Butylbenzane 0.50 u
98-06-6 tert-Butvlbenzene 0.50 u
56-23-5 Carbon tetrachloride 0.50 u
I 108-90-7 Chiaro benzene 0.50 u
75-00-3 Chloroethane 0.50 u
67-66-3 Chloroform 0.50 u
74-87-3 Chiaro methane 0.50 u
I 95-49-8 2-Chlorotoluene 0.50 u
106-43-4 4-Chlorotoluene 0.50 u
124-48-1 Oibromochloromethane 0.50 u
96-12-8 1,2-Dibromo-3-chioroprooane 0.50 u
I 1 06-93-4 1 ,2-Dibromoethane 0.50 u
74.95.3 Oibromomethane 0.50 u
95-50-1 1 ,2-Dichlorobenzene 0.50 u
541-73-1 1,3-0ichlorobenzene 0.50 u
I 106-46-7 1 ,4-Dichlorobenzene 0.50 u
75-71-8 Dichlorodifluoromethane 0.50 u
75.34.3 1, 1-Dichloroethane 0.50 u
107-06-2 1,2-0ichloroethane 0.50 u
I 75.35.4 1, 1-0ichloroethene 0.50 u
156-59-4 cis-1,2-Dichloroethene 0.50 u
156-60-5 trans-1 ,2-0ichloroethene 0.50 u
I 78-87-5 1,2-Dichloropropane 0.50 u
142-28-9 1.3-0ichlorooropane 0.50 u
590-20-7 2. 2 -Dichloropropane 0.50 u
563-58-6 1, 1-0ichloropropene 0.50 u
I 10061-01-5 cis-1 ,3-Dichloropropene 0.50 u
10061-02-6 trans-1 ,3-Dichloropropene 0.50 u
100-41-4 Ethyl benzene 0.50 u
87-68-3 Hexachlorobutadiene 0.50 u
I 98-82-8 lsopropylbenzene 0.50 u
99-87-6 4-lsopropyttoluene 0.50 u
75-09-2 Methylene chloride 0.50 u
91-20-3 Naphthalene 0.50 u
I 103-65-1 Propylbenzene 0.50 u
100-42-5 Styrene 0.50 u
630-20-6 1.1, 1.2-Tetrachloroethane 0.50 u
79.34.5 1, 1 ,2,2· Tetrachloroethane 0.50 u
I 127-18-4 Tetrachloroethene 0.50 u
108-88-3 Toluene 0.50 u
87-61-6 1 ,2,3-Trichlorobenzene 0.50 u
120-82-1 1,2.4-Trichlorobenzene 0.50 u
I 71-55-6 1, 1, 1-Trichloroethane 0.50 u
79-00-5 1, 1,2-Trichloroethane 0.50 u
79-01-6 Trichloroethane 0.50 u
75-69-4 T richlorofluoromethane 0.50 u I 96-18-4 1,2,3-Trichloroprooane 0.50 u
95-63-6 1,2,4-Trimethylbenzene 0.50 u
108-67-8 1,3,5-Trimethvlbenzene 0.50 u
I 75-01-4 Vinyl chloride 0.50 u
Total Xvlenes 0.50 u 052
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1A SAMPLE NO.
502.2 ANALYSIS DATA SHEET
Lab Name: IEA-FL ---------------
Project No.: 09:.5:.·..:0.;.7..;1..:2 _____ _
Matrix: (soil/water)
Lev1!I: (low/med)
Dilujon Factor:
CAS No
71-43-2
108-86-1
74.97.5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74.95.3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
1 07-06-2
75.35.4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79.34.5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
WATER
LOW
1.0
Compound
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bro mo methane
n-Butylbenzene
sec-Butv!benzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Oibromochloromethane
1.2-0ibromo-3-chlorooropane
1,2-Dibromoethane
Oibromomethane
1,2-Dichlorobenzene
1 ,3-0ichlorobenzene
1,4-0ichlorobenzene
Oichlorodifluoromethane
1, 1-0ichloroethane
1,2-0ichloroethane
1, 1-0ichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2 .2-Dichloropropane
1, 1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-0ichloropropene
Ethyl benzene
Hexachlorobutadiene
lsopropylbenzene
4-lsopropyltoluene
Methylene chloride
Naphthalene
Propylbenzene
Styrene
1, 1, 1,2-Tetrachloroethane
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1 ,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1 ,2,3-Trichloroprooane
1 ,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
Total Xylenes
LAMBERT
Lab Sample ID: LAMBERT
Lab File ID:..:7_;1..:2..:L ___ _
Date Sampled: ..:3::.16;;;1..:9..:5 ___ _
Date Analyzed: ..:3::.1.:.14.;:l..:9..:5 __ _
Concentration Units:
{ug/L or ug/Kg) ug/1 Q
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
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1A SAMPLE NO.
502.2 ANALYSIS DATA SHEET
Lab Name: IEA-FL ------------
Proj1~ct No.: 09:..:5:..·.::0.:.7.:.1.::2 _____ _
Matoix: !soil/water)
Levtd: (low/med)
Dilution Factor:
CAS No
71-43-2
1 08-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
1 03-65-1
1 00-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
WATER
LOW
1.0
Compound
Benzene
Bromobenzene
Bromochloromethane
Bro modi chl o ro m ethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-8U1ylbenzene
Carbon tetrachloride
Ch/orobenzene
Chloroethane
Chloroform
Chloromethane
2-Chiorotoluene
4-Chlorotoluene
Dibromochloromethane
1 ,2-Dibromo-3-ch!oropropane
1 ,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1.3-Dichlorobenzene
1,4-Dichlorobenzene
Oich!orodifluoromethane
1, 1-0ichloroethane
1 ,2-0ichloroethane
1, 1-0ichloroethene
cis-1,2-0ichloroethene
trans-t ,2-0ich!oroethene
1,2-0ichloropropane
1,3-0ichloropropane
2,2-0ichloropropane
1, 1-0ichloropropene
cis-1,3-0ichloropropene
trans-1,3-0ichlorooropene
Ethylbenzene
Hexachlorobutadiene
lsopropylbenzene
4-lsopropyltoluene
Methylene chloride
Naphthalene
Propyibenzene
Styrene
1, 1, 1,2-Tetrachloroethane
1, 1 ,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1 ,2, 3-Trichlorobenzene
1 ,2,4-Trichlorobenzene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
T richlorofluoromethane
1,2,3-Trichloroprooane
1,2,4-Trimethylbenzene
1 ,3, 5-Trimethylbenzene
Vinyl chloride
Total Xylenes
MARTIN
Lab Sample JD: MARTIN
Lab File !D: 07_;1..:2;;;M _____ _
Date Sampled: ~3c./.:;6/..:9..:5 ___ _
Date Analyzed: 3/14/95
Concentration Units:
(ug/L or ug/Kg) ug/I Q
1.3
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 I u
0.50 u
7.8
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
054
1A SAMPLE NO.
I 502.2 ANALYSIS OATA SHEET
Lab Name: IEA-FL
I
WALKER
I
Proj ~c:: No.: · ~9:..;5;..·.::0c.7_1.;;2 _____ _
Mat:ix: (soil/water) WATER
Lab Sample ID: WALKER
Lab File ID: 712W
Level: (low/med) LOW Date Sampled: 316195
I Dilution Factor: 1.0 Date Analyzed: 3114195
Concentration Units:
CAS No Compound (ug/l or ug/Kg) ug/1 Q
I 71-43-2 Benzene 0.50 u
108-86-1 Brom a benzene 0.50 u
74-97-5 Bromochloromethane 0.50 u
I 75-27-4 Bromodichloromethane 0.50 u
75-25-2 Bromoform 0.50 u
74-83-9 Bromomethane 0.50 u
104-51-8 n-Buty/benzene 0.50 u
I 135-98-8 sec-Butylbenzene 0.50 u
98-06-6 tert-Butylbenzene 0.50 u
56-23-5 Carbon tetrachloride 0.50 u
108-90-7 Chlorobenzene 0.50 u
I 75-00-3 Chloroethane 0.50 u
67-66-3 Chloroform 0.50 u
74-87-3 Chloromethane 0.50 u
95-49-8 2-Ch!orotoluene 0.50 u
I 106-43-4 4-Chlorotoluene 0.50 u
124-48-1 Oibromochloromethane 0.50 u
96-12-8 1 ,2-Dibromo-3-ch!oropropane 0.50 u
I 106-93-4 1,2-Dibromoethane 0.50 u
74-95-3 Dibromomethane 0.50 u
95-50-1 1,2-Dichlorobenzene 0.50 u
541-73-1 1,3-0ichlorobenzene 0.50 u
I 1 06-46-7 1 ,4-Dichlorobenzene 0.50 u
75-71-8 Oich!orodiftuoromethane 0.50 u
75-34-3 1, 1-Dichloroethane 0.50 u
107-06-2 1,2-0ichloroethane 0.50 u
I 75-35-4 1, 1-0ichloroethene 0.50 u
156-59-4 cis-1,2-Dichloroethene 0.50 u
156-60-5 trans-1,2-Dichloroethene 0.50 u
78-87-5 1,2-Dichloropropane 0.50 u
I 142-28-9 1, 3-Dichloropropane 0.50 u
590-20-7 2, 2-Dichloropropane 0.50 u
563-58-6 1, 1-Dichloropropene 0.50 u
10061-01-5 cis-1,3-Dich!oropropene 0.50 u
I 1 0061-02-6 trans-1 ,3-Dichloropropene 0.50 u
100-41-4 Ethy!benzene 0.50 u
87-68-3 Hexachlorobutadiene 0.50 u
98-82-8 lsopropylbenzene 0.50 u
I 99-87-6 4-lsopropyltoluene 0.50 u
75-09-2 Methylene chloride 0.50 u
91-20-3 Naphthalene 0.50 u
103-65-1 Propylbenzene 0.50 u
I 100-42-5 Styrene 0.50 u
630-20-6 1, 1, 1 ,2-Tetrachloroethane 0.50 u
79-34-5 1, 1,2,2-Tetrachloroethane 0.50 u
127-18-4 T etrachloroethene 0.50 u
I 108-88-3 Toluene 0.50 u
87-61-6 1,2.3-Trichlorobenzene 0.50 u
120-82-1 1,2,4-Trichlorobenzene 0.50 u
I 71-55-6 1, 1, 1-Trichloroethane 0.50 u
79-00-5 1, 1,2-Trichloroethane 0.50 u
79-01-6 Trichloroethane 0.50 u
75-69-4 T richlorofluoromethane 0.50 u
I 96-18-4 1,2,3-Trichloropropane 0.50 u
95-63-6 1,2,4-Trimethylbenzene 0.50 u
108-67-8 1 ,3,5-Trimethylbenzene 0.50 u
I
75-01-4 Vinyl chloride 0.50 u
Total Xylenes 0.50 u 055
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1A SAMPLE NO.
502.2 ANALYSIS DATA SHEET I TRIP BLANK Lab Name: IEA-FL -=------------
Project No.: ..:9..:5:..·;;.0.:.7.:.1:;.2 _____ _
Matrix: (soil/water}
Lev1~I: (low/med)
Dilution Factor:
CAS No
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
1 20-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
WATER
LOW
1.0
Compound
Benzene
Bromobenzene
Bromochloromethane
Bromodich!oromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Ch!orotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromo-3-chloropropane
1,2-0ibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1 ,4-0ichlorobenzene
Dichlorodifluoromethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1 •0ichloroethene
cis-1,2-Dichloroethene
trans• 1 ,2•Dichloroethene
1 ,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1, 1-Dichlorooropene
cis-1,3-Dichloropropene
trans-1 ,3-Dichloropropene
Ethylbenzene
Hexachtorobutadiene
lsopropy!benzene
4-lsopropyltoluene
Methylene chloride
Naphthalene
Propylbenzene
Styrene
1, 1, 1,2-Tetrachloroethane
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1 ,2,3-Trichlorobenzene
1 ,2,4-Trichlorobenzene
1, 1, 1-Trich!oroethane
1, 1,2-Trich!oroethane
Trichloroethane
T richlorof luoromethane
1 ,2, 3-Trich!oroprooane
1 ,2,4-Trimethvtbenzene
1 ,3, 5-Trimethylbenzene
Vinyl chloride
Total Xylenes
Lab Sample ID: TRIP BLANK
Lab File ID: .:.7.:.1:;.2T.:.;B:..._ __ _
Date Sampled: ..:3::.i6:::i..:9..:5c_ __ _
Date Analyzed: ..:3::.11.:.4.::i..:9..:5 __ _
Concentration Units:
(ug/L or ug/Kgl ug/1 Q
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u
0.50 u 056
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Lab Name: IEA-FL
Project No.: 95-0712
Matrix: !soil/water)
Level: !low/med)
Dilution Factor:
CAS No.
208-%-8
15972-60-8
309-00-2
120-12-7
1912-24-9
56-55-3
205-82-3
207-08-9
50-32-8
191-24-2
85-68-7
5103-71-9
5103-74-2
39765-80-5
2051-130-7
218-0'1-9
53-70-3
84-72-2
16605-91-7
84-66-2
103-23-1
117-81-7
131-11-3
72-20-:3
86-73-7
76-44-13
1024-57-3
52663-71-5
118-74-1
60145-22-4
77-47-4
193-39-5
58-89-~I
I L-4-1-C•
40186-71-8
60233-:25-2
87-86-5
85-01-8
129-00-0
122-34-9
2437-711-8
15862-07-4
1A SAMPLE NO.
525.1 ANALYSIS DATA SHEET
WATER
LOW
1.0
Compound
Acenaphthylene
Alachlor
Aldrin
Anthracene
Atrazine
Benzo[a]anthracene
Benzo[b ]fluoranthene
Be nzo [ k I flu ora nthe ne
Benzo[a]pyrene
Benzo[g,h ,i]perylene
Butyl be nzyl ph tha I ate
alpha-chlordane
gamma-chlordane
trans nonachlor
2-Chlorobiphenyl
Chrysene
Dibenz[a ,h]anthracene
Di-n-butylphthalate
2, 3-Dichlorobiphenyl
Diethylphthalate
Bis( 2-ethylhexyl) adipate
Bis( 2-ethylhexyl) phthalate
Dimethylphthalate
Endrin
Fluorene
Heptachlor
Heptachlor epoxide
2,2' ,3,3' ,4,4', 6-Heptachlorobiphenyl
Hexachlorobenzene·
2,2' ,4,4' ,5,6'-Hexachlorobiphenyl
Hexachlorocyclopentadiene
lndeno[1,2,3,c,d]pyrene
Lindane
1v1etnoxycn1or
2, 2' ,3.3' ,4, 5' ,6.6' -Octach!orobiphenyl
2. 2', 3' ,4, 6-Pentachlorobiphenyl
Pentachlorophenol
Phenanthrene
Pyrene
Simazine
2, 2' ,4,4' -Tetrachlorobiphenyl
2 ,4, 5-Trichlorobiphenyl
Lab Sample ID: ELLIOT
Lab File ID: ELLIOT
Date Sampled: 3/6/95
Date Extracted: 3/11 /95
Date Analyzed: 3/11 /95
Concentration Units:
lug/L or ug/Kg) ug/L Q
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1 .0 u
1 .0 u
1 .0 u
1.0 u
1.0 u
1 .o . u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1 .o u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.U u
1 .0 u
1 .o u
1 .0 u
1 .0 u
1.0 u
1 .o u
1.0 u
1.0 u
ELLIOT
I 41
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Lab Name: IEA-FL
Project No.: 95-0712
Matrix: (soil/water)
Level: (low/med)
Dilution Factor:
CAS No.
208-96-8
15972-60-8
309-00-2
1 20-·1 2-7
1912-24-9
56-5E;-3
205-f:2-3
207-08-9
50-32-8
191-24-2
85-68-7
5103-71-9
5103-74-2
39765-80-5
2051-130-7
218-0'1-9
53-70-3
84-72-2
16605-91-7
84-66-2
103-23-1
117-81-7
131-11-3
72-20-B
86-73-7
76-44-8
1024-57-3
52663-71-5
118-74-1
60145-22-4
77-47-4
193-39-5
58-89-9
U-4<!-~
40186-71-8
60233-25-2
87-86-5
85-01-8
129-00-0
122-34-9
2437-79-8
15862-07-4
1A SAMPLE NO.
525.1 ANALYSIS DATA SHEET
WATER
LOW
1 .0
Compound
Acenaphthylene
Alachlor
Aldrin
Anthracene
Atrazine
Benzo[a ]anthracene
Benzo[b ]fluoranthene
Be nzo [ k !flu o ranthene
Benzo[ajpyrene
Benzo[g, h ,i]perylene
Butylbe nzyl p hth al ate
alpha-chlordane
gamma-chlordane
trans nonachlor
2-Chlorobiphenyl
Chrysene
Dibenz[a ,h ]anthracene
Di-n-butylphthalate
2 ,3-Dichlorobiphenyl
Diethylphthalate
Bis( 2-ethylhexyl) adipate
Sis I 2-ethyl he xyl Ip hthalate
Dimethylphthalate
Endrin
Fluorene
Heptachlor
Heptachlor epoxide
2,2' ,3,3' ,4,4' ,6-Heptachiorobiphenyl
Hexachlorobenzene
2,2' ,4.4 ·, 5, 6 · -Hexachlorobiphenyl
Hexachlorocyclopentadiene
lndeno[1,2,3,c,d)pyrene
Lindane
,v,etnoxycnfor
2,2' ,3,3' ,4, 5 · ,6,6' -Octachlorobiphenyl
2, 2', 3' ,4, 6-Pentachlorobiphenyl
Pentachlorophenol
Phenanthrene
Pyrene
Simazine
2,2' ,4,4' -Tetrachlorobiphenyl
2, 4, 5-Trichlorobiphenyl
LAMBERT
Lab Sample ID: LAMBERT
Lab File ID: LAMBERT
Date Sampled: 3/6/95
Date Extracted: 3/11 /95
Date Analyzed: 3/11 /95
Concentration Units:
Jug/L or ug/Kg) ug/L Q
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1 .0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1 .0 u
l .U u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
042
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1A SAMPLE NO.
525.1 ANALYSIS DATA SHEET
MARTIN
Lab Name: IEA-FL _;_::;,_c,_:;__ __________ _
Project No.: 95-0712
Matrix: (soil/water)
Level: (low/med)
Dilution Factor:
CAS No.
208-B6-8
15972-60-8
309-00-2
120-12-7
1912-24-9
56-55-3
205-82-3
207-08-9
50-32·8
191-24-2
85-68--7
5103-71-9
5103-74-2
39765-80-5
2051-EiO-7
218-01-9
53-70-3
84-72-.2
16605-91-7
84-66-2
103-23-1
117-81-7
1 31 -11 -3
72-20-E:
86-73-7
76-44-8
1024-57-3
52663-71-5
118-74-1
60145-22-4
77-4 7-4
193-39-5
58-89-9
I L·4J·b
40186-71-8
60233-25-2
87-86-5
85-01-8
129-00-0
122-34-~I
2437-79-·8
15862-07-4
WATER
LOW
1.0
Compound
Acenaphthylene
Alachlor
Aldrin
Anthracene
Atrazine
Benzo(a]anthracene
Benzo(b ]fluoranthene
Be nzo I k If I uora nthe ne
Benzo(a]pyrene
Be nzo (g, h, i] peryle ne
Butyl be nzyl p hthal ate
alpha-chlordane
gamma-chlordane
trans nonachlor
2-Chlorobiphenyl
Chrysene
Di benz( a, h I anthrace ne
Di-n-butylphthalate
2, 3-Dichlorobiphenyl
Diethylphthalate
Bis( 2-ethylhexyl) adipate
Bis(2-ethylhexyl)phthalate
Dimethylphthalate
Endrin
Fluorene
Heptachlor
Heptachlor epoxide
2,2' ,3,3' ,4.4' ,6-Heptachlorobiphenyl
Hexachlorobenzene
2,2' ,4,4', 5, 6' -Hexachlorobiphenyl
Hexachlorocyclopentadiene
lndeno(1,2,3,c,d]pyrene
Lindane
,v,etnoxycnior
2,2' ,3, 3' ,4,5', 6,6'-0ctachlorobiphenyl
2,2' ,3' ,4,6-Pentachlorobiphenyl
Pentachlorophenol
Phenanthrene
Pyrene
Simazine
2,2' ,4,4' -Tetrachlorobiphenyl
2,4, 5-Trichlorobiphenyl
Lab Sample ID: MARTIN
Lab File ID: MARTIN
Date Sampled: 3/6/95
Date Extracted: 3/11 /95
Date Analyzed: 3/11/95
Concentration Units:
(ug/L or ug/Kg) ug/L Q
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1 .o u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
I.U u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
.
43
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1A SAMPLE NO.
525.1 ANALYSIS DATA SHEET
Lab Name: IEA-FL _:.::;_:__:_=-------------
Project No.: 95-0712
Matrix: (soil/water) WATER
Level: (low/med) LOW
Dilution Factor: 1.0
CAS No. Compound
208-96-8 Acenaphthylene
1597.2-60-8 Alachlor
309-00-2 Aldrin
120-12-7 Anthracene
1912-24-9 Atrazine
56-55-3 Benzo[a ]anthracene
205-82-3 Benzo[b ]fluoranthene
207-08-9 Benzo[ k If I uoranthe ne
50-32-8 Benzo[a]pyrene
191-24-2 Benzo[g ,h ,i]perylene
85-68--7 Butyl be nzylphth al ate
5103-71-9 alpha-chlordane
5103-74-2 gamma-chlordane
39765-80-5 trans nonachlor
2051-fiO-7 2-Chlorobiphenyl
21 8-0·, _9 Chrysene
53-70-3 Dibe nz[ a, h I a nthra ce ne
84-72-2 Di-n-butylphthalate
16605--91-7 2, 3-Dichlorobiphenyl
84-66-2 Diethylphthalate
103-23-1 Bis( 2-ethylhexyll adipate
117-81-7 Bis( 2-ethylhexyll phthalate
131-11-3 Dimethylphthalate
72-20-H Endrin
86-73-7 Fluorene
76-44-B Heptachlor
1024-5 7-3 Heptachlor epoxide
52663-71-5 2,2' ,3,3' ,4,4' ,6-Heptachlorobiphenyl
118-74--1 Hexachlorobenzene
60145-:22-4 2,2' ,4,4 ·, 5, 6" -Hexachlorobiphenyl
77-4 7-4 Hexachlorocyclopentadiene
193-39-5 lndeno[l ,2,3,c,d]pyrene
58-89-9 lindane
, ,-4;;-, 1v1emoxycn1or
40186-71-8 2,2' ,3, 3' ,4, 5' ,6,6' -Octachlorobiphenyl
60233-25-2 2, 2', 3' ,4, 6-Pentachlorobiphenyl
87-86-5 Pentachlorophenol
85-01 -8 Phenanthrene
129-00-0 Pyrene
122-34-9 Simazine
2437-79-8 2,2' ,4,4' -Tetrachlorobiphenyl
15862-07-4 2, 4, 5-Trichlorobiphenyl
STEIN
Lab Sample ID: _S_T_E_IN __ _
Lab File ID: STEIN -----
Date Sampled: 3/6/95
Date Extracted: 3/11 /95
Date Analyzed: 3/11 /95
Concentration Units:
(ug/L or ug/Kg) ug/L Q
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1 .0 u
1 .0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 · u
1.0 u
1.0 u
1 .0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
I.U u
1.0 u
1 .0 u
1 .o u
1.0 u
1 .o u
1 .o u
1 .0 u
1.0 u
-
u 44
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Lab Name: IEA-FL
Project No.: 95-0712
Matrix: (soil/water)
Level: (low/med)
Dilution Factor:
CAS No.
208-96-8
15972-60-8
309-00-2
120-12-7
1912-24-9
56-55-3
205-82-3
207-08-9
50-32-8
191-24-2
85-68--7
5103-71-9
5103-74-2
39765-80-5
2051-60-7
218-01-9
53-70-3
84-72-2
16605-91-7
84-66-2
103-23-1
117-81-7
131-11-3
72-20-El
86-73-7
76-44-E:
1024-57-3
52663-71-5
118-74-1
60145-22-4
77-47-4
193-39-5
58-89-9
I~-~~-';)
40186-71-8
60233-25-2
87-86-5
85-01-8
1 29-00-0
122-34-11
2437-79-8
15862-07-4
1A SAMPLE NO.
525.1 ANALYSIS DATA SHEET
WATER
LOW
Compound
Acenaphthylene
Alachlor
Aldrin
Anthracene
Atrazine
Benzo[a]anthracene
Benzo[b ]fluoranthene
Be nzo [k ]f I uora nthene
Benzo(a]pyrene
Benzo[g ,h ,i]perylene
Butyl benzyl phtha I ate
alpha-chlordane
gamma-chlordane
trans nonachlor
2-Chlorobiphenyl
Chrysene
Dibenz[a ,h ]anthracene
Di-n-butylphthalate
2,3-Dichlorobiphenyl
Diethylphthalate
Bis(2-ethylhexyl) adipate
Bis I 2-ethyl hexyl Ip hth al ate
Dimethylphthalate
Endrin
Fluorene
Heptachlor
Heptachlor epoxide
2,2' ,3,3' ,4,4' ,6-Heptachlorobiphenyt
Hexachlorobenzene
2, 2 · ,4.4', 5, 6" -Hexachlorobiphenyl
Hexachlorocyclopentadiene
lndeno[1,2,3,c,d]pyrene
Lindane
1v,etnoxycn1or
2.2' ,3.3' ,4,5' ,6,6' -Octachlorobiphenyl
2, 2', 3' ,4, 6-Pentachlorobiphenyl
Pentachlorophenol
Phenanthrene
Pyrene
Simazine
2,2' ,4,4' -Tetrachlorobiphenyl
2, 4, 5-T richlorobiphenyl
Lab Sample ID: WALKER
Lab File ID: WALKER
Date Sampled: 3/6/95
Date Extracted: 3/11 /95
Date Analyzed: 3/11 /95
Concentration Units:
(ug/L or ug/Kg) ug/L Q
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1 .0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
I.U u
1.0 u
1 .0 u
1 .o u
1 .0 u
1 .0 u
1.0 u
1.0 u
1.0 u
WALKER
.
045
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lab Name: IEA-Fl
Project No.: 95-0712
Matrix: (soil/water)
Level: (low/med)
Dilution Factor:
CAS No.
5972-60-8
309-00-2
1912-24-9
57-74-9
60-57-1
72-20--8
76-44-8
1024-!j7-3
118-74-1
77-74-4
58-89-9
72-43-5
122·3~--9
8001-:::5-2
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-92-5
1A SAMPLE NO.
505 ANALYSIS DATA SHEET
WATER
LOW
1.0
Compound
Alachlor
Aldrin
Atrazine
Chlordane
Dieldrin
Endrin
Heptachlor
Heptachlor epoxide
Hexachlorobenzene
Hexachlorocyclopentadiene
Lindane
Methoxychlor
Simazine
Toxaphene
PCB1016
PCB 1221
PCB 1232
PCB 1242
PCB 1248
PCB 1254
PCB 1260
ELLIOT
lab Sample ID: ELLIOT ------
lab File ID: 5050311 .04
Date Sampled: 3/6/95 ------
Date Extracted: 3/9/95 ------
Date Analyzed: 3/11 /95
Concentration Units:
(ug/l or ug/Kg) ug/I Q
-
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.10 u
0.10 u
0.10 u
0.10 u
0.10 u
0.10 u
0.10 u
0.10 u
0.10 u
046
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Lab Name: IEA-FL
Project No.: !35-0712
Matrix: (soil/water)
Level: (low/med)
Dilution Factor:
CAS No.
5972-60-8
309-00-2
1912-24-9
57-74-9
60-57-1
72-20-8
76-44-8
1024-57-3
118-74-1
77-74-4
58-89-9
72-43-5
122-34-9
8001-:35-2
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
1A SAMPLE ND.
505 ANALYSIS DATA SHEET
WATER
LOW
1.0
Compound
Alachlor
Aldrin
Atrazine
Chlordane
Dieldrin
Endrin
Heptachlor
Heptachlor epoxide
Hexachlorobenzene
Hexachlorocyclopentadiene
Lindane
Methoxychlor
Simazine
Toxaphene
PCB 1016
PCB 1221
PCB 1232
PCB 1242
PCB 1248
PCB 1254
PCB 1260
STEIN
Lab Sample ID: ..:S;..;T..:E;;.;IN_:_ __ _
Lab File ID: 5050311.041
Date Sam p I e d: ..:3;.;./6.:c/..:9..:5 ___ _
Date Extracted: 3/9/95 ...:.:..;:.:....::..::__ __
Date Analyzed: ..:3;.;./1.:..1.:../.=9.=5 __ _
Concentration Units:
(ug/L or ug/Kg) ug/1 Q
-0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.10 u
0.10 u
0.10 u
0.10 u
0.10 u
0.10 u
0.10 u
0.10 u
0.10 u
047
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Lab Name: IEA-FL
Project No.: 95-0712
Matrix: (soil/water)
Level: (lowimed)
Dilution Factor:
CAS No.
5972-60-8
309-00-2
1912 .. 24-9
57-74-9
60-57-1
72-20-8
76-44-8
1024-57-3
118-7'1--1
77_74 .. 4
58-89 .. 9
72-43-5
122-34-9
8001 <35-2
12674-11-2
11104-28-2
11141 .. 16-5
53469--21-9
12672-29-6
11097-69-1
11096-82-5
1A SAMPLE NO.
505 ANALYSIS DATA SHEET
WATER
LOW
1.0
Compound.
Alachlor
Aldrin
Atrazine
Chlordane
Dieldrin
Endrin
Heptachlor
Heptachlor epoxide
Hexachlorobenzene
Hexachlorocyclopentadiene
lindane
Methoxychlor
Simazine
Toxaphene
PCB 1016
PCB 1221
PCB 1232
PCB 1242
PCB 1248
PCB 1254
PCB 1260
LAMBERT
Lab Sample ID: LAMBERT
Lab File ID: 5050311 .042
Date Sampled: 3/6/95 ------
Date Extracted: 3/9/95 ------
Date Analyzed: 3/11 /95 ------
Concentration Units:
(ug/L or ug/Kg) ug/I Q
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.010 u
0.10 u
0.10 u
0.10 u
0.10 u
0.10 u
0.10 u
0.10 u
0.10 u
0.10 u
048
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Lab Name: IEA-FL
Project No.: 95-0712
Matrix: (soil/water}
Level: (low/med)
Dilution Factor:
CAS No.
5972-60-8
309-00-2
1912-24-9
57_74 .. 9
60-57·1
72-20-8
76-44-8
1024-Ei7-3
118-7~--1
77-74-4
58-89-:3
72-43-!3
122-34-9
8001-35-2
12674-11-2
11104-28-2
11141-16-5
53469-.21-9
12672-:29-6
11097-69-1
11096-B2-5
1A SAMPLE NO.
505 ANALYSIS DATA SHEET
WALKER
Lab Sample ID: WALKER
WATER Lab File ID: 5050311 .044
LOW Date Sampled: _3_/6_/_9_5 ___ _
1.0 Date Extracted: 3/9/95 ....;._,;_;, ___ _
Date Analyzed: 3/11 /95
Concentration Units:
Compound (ug/L or ug/Kg} ug/1 Q
Alachlor 0.010 u
Aldrin 0.010 u
Atrazine 0.010 u
Chlordane 0.010 u
Dieldrin 0.010 u
Endrin 0.010 u
Heptachlor 0.010 u
Heptachlor epoxide 0.010 u
Hexachlorobenzene 0.010 u
Hexachlorocyclopentadiene 0.010 u
Lindane 0.010 u
Methoxychlor 0.010 u
Simazine 0.10 u
Toxaphene 0.10 u
PCB 1016 0.10 u
PCB 1221 0.10 u
PCB 1232 0.10 u
PCB 1242 0.10 u
PCB 1248 0.10 u
PCB 1254 0.10 u
PCB 1260 0.10 u
050
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Project No.: 619-690 TCLP fraction missing
The 8240 part of this project came through data review as normal and was final reviewed on
March 24, 1995. The data for project sheet apparently was not checked for test codes other than
the 8240 test code by the initial or final reviewers. Upon investigation as to where the sample
was analyzed it was found that the sample was on the lab's sams list on Friday March 24, 1995
but not on the sams list on Monday March 27, 1995. Apparently the sample was marked in
sams as completed by the laboratory between the 24th and the 27th of March. For this reason
the laboratory thought the sample was analyzed and therefore did not analyze the sample at all.
In addition the samples could not be found in the storage refrigerator to be analyzed past the
method specified holding time (this may have changed since we first looked).
Brian D. Neptune
Lead Analyst, GC/MS Final Review
April 14, 1995
002
+B-6 88t. Bo--'-. . 'P?-57
tc.Jihs-c§'-G~
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IEA SDG NARRATIVE SEMIVOLATILE FRACTION
PROJECT: 619-690 BATCH: 03208 METHOD: SW-8468270TCLP
Samples: ( 1) Leachate
The samples were received at Industrial and Environmental Analysts, Inc. (IEA) on March 10, 1995.
The temperature upon receipt was 4°C. Each sample was assigned a 9-character "IEA" lab identification
number (lab ID) and an abbreviated client ID which is referenced on the !EA Assigned Number Index.
All analyses are performed in accordance with EPA approved methodologies and meet the requirements
of the mA Quality Assurance Program. Please see the enclosed data package for your results and Chain
of Custody documentation.
The chromatographic separation of the analytes was performed using a Restek 30 X 0.32 XTI-5 fused
silica capillary column with a 0.5 µ.m bonded phase film thickness.
Instrument data printouts identify the compound 2 ,2 '-oxybis(l-Chloropropane) with CAS number 108-60-
1. Alternative nomenclature for this compound is bis(2-Chloroisopropyl)ether which is included on repon
forms submitted.
The "J" flag indicates an estimated concentration below the quantitation limit and reported to 2.0 ng on
coltllilil.
The "M" flag used on the data system report form designates that a manual integration was required to
provide im accurate quantification of that analyte. Manual integrations have been initialed and dated by
the analyst.
The acid surrogates did not recover within method specified limits in sample SRB (950320801). This
is due to suspected matrix interference and has been confirmed by analysis and extraction of the matrix
spike, SRBSPK (950320801SPK).
I certify that this data package is in compliance with the procedures and methods defined for this project,
both technically and for completeness, for other than the conditions detailed above. Release of the data
contained in this bartlcopy data. package and in the computer-readable data (if applicable) as submitted
bas been authorized by the laboratory manager or his designee, as verified by the following signature.
Dawn A. Casto
GC/MS Data Reviewer
IEA, Inc.
IEA. lo: Ooc.f RPF00701.NC
03/28/95
1
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IEA SDG NARRATIVE PESTICIDE FRACTION
PROJECT:619-690 SDG:03208 METHOD:8080TCLP/8150TCLP/8080
Samples: (1) Soil Sample
The samples were received at Industrial and Environmental Analysts, Inc. (IEA) on March 09, 1995.
Each sample was assigned a 9-character "IEA" lab identification number (lab ID) and an abbreviated
client ID which is referenced on the IEA Assigned Number Index. All analyses are performed in
accordance with EPA approved methodologies and meet the requirements of the IEA Quality Assurance
Progran1. Please see the enclosed data package for your results and Chain of Custody documentation.
The chromatographic separation of the analytes was performed using a J & W 30 m X 0.53 mm DB-1701
fused silica capillary column with a 1.0 /Lm bonded phase film thickness and a Restek 30 m X 0.53 mm
Rtx-35 fused silica capillary column with a 1.0 /Lm bonded phase film thickness.
Any nonconformances associated with the analysis of the samples in this project are as follows:
The Matrix Spike/Matrix Spike Duplicate (MS/MSD) for the Pesticide 8080 analysis did not meet the
method c:riteria for all compounds due to sample matrix interference and sample dilution. Therefore, the
Laboratory Control Sample (LCS) has been reported. Endosulfan I is above the method limits in the LCS
and delta.-BHC is below the limits due to degradation of the spiking standard solution. Neither of these
compounds is reported in the sample. The extract for the Pesticide 8080 analysis was analyzed at a !OX
dilution clue to non-target compounds that exceeded the calibration range.
The TCLP 8080 and TCLP 8150 analyses proceeded with no deviations from the method.
I certify that this data package is in compliance with the procedures and methods defined for this project,
both tech.nically and for completeness, for other than the conditions detailed above. Release of the data
contained in this hardcopy data package and in the computer-readable data (if applicable) as submitted
has been authorized by the laboratory manager or his designee, as verified by the following signature.
'l.J.....l,;~~:=.:· ""·,ct ....... ~~.1.:.<"'\_.5D=:,:>.=
0
::...>.... ___ 03;29;95
Katrina L Travis
GC Supervisor
IEA, Inc.
IEA. Inc !loci RPFOOSOI.NC
1
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IEA SDG NARRATIVE INORGAi"IIC/METALS FRACTION
REVISED CASE NARRATIVE
CASE: 619 687 SDG NO.: 3195 CONTRACT: NI A
Samples: 950319714 (FP) for TCLP Metals Analysis
This case was closed on March 8, 1995. The temperature of the samples upon receipt by [ndustrial and
Environmental Analysts, Inc. (IEA) was 4"C. All samples were received intact.
This project was divided into two reports due to the different reporting limits for the leachates and
software limitations.
The pH of sample FP was7 .57 before the leaching process began. The sample was leached at a pH of
4.93, and preserved for storage at a pH less than two.
Sample CL2 is included in this SDG as it was used for the ICP serial dilution.
Each sample has been assigned a 9-character !EA lab identification number.
Any nonconformances associated with the analysis of samples in this case are noted as follows: Sample
FP was releached for mercury analysis due to a failed matrix spike. The analysis from 3/ l 7 /95 is included
to show the reason for releaching.
I certify that this data package is in compliance with the terms and conditions of the contract, both
technically and for completeness, for other than the conditions detailed above. Release of the data
contained in this hardcopy data package and in the computer-readable data submitted on diskette has been
authorized by the laboratory manager or his designee, as verified by the following signature.
Inorganic Data Reviewer
IEA, Inc.
IEA, Inc Doc# RPF00900.NC
1
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IEA SDG NARRATIVE INORGANIC/l'vIETALS FRACTION
REVISED CASE NARRATIVE
CASE: 619 690 SDG NO.: 03208 CONTRACT: NIA
Sample1;: One leachate sample, 950320801 (SBR), for TCLP Metals Analysis.
This case was closed on March 9, 1995. The temperature of the samples upon receipt by Industrial and
Environmental Analysts, Inc. (!EA) was 3°C. All samples were received intact.
This project was divided into two separate reports due to the different reporting limits for the leachates
and software limitations.
The pH of TCLP sample SBR for Metals analysis was less than two (2) at the time of sample preparation.
Each sample has been assigned a 9-character !EA lab identification number.
The "E" flag is used· on Form 1 to identify a value that is estimated due to the presence of an
interference. From the data available, there is no obvious explaination for the "E" flag on barium.
I certify that this data package is in compliance with the terms and conditions of the contract, both
technically and for completeness, for other than the conditions detailed above. Release of the data
contained in this hardcopy data package and in the computer-readable data submitted on diskette has been
authorized by the laboratory manager or his designee, as verified by the following signature.
W<-Edt-£ 612195
Inorganic Data Reviewer
!EA, Inc.
!EA, Inc Doc# :~PF00900.NC
1
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IEA SDG NARRATIVE INORGANIC/l\-lETALS FRACTION
REVISED CASE NARRATIVE
CASE: 619 690 SDG NO.: 03208 CONTRACT: NIA
Samples: One leachate sample, 950320801 (SBR), for TCLP Metals Analysis.
This case was closed on March 9, 1995. The temperature of the samples upon receipt by Industrial and
Environmental Analysts, Inc. (IEA) was 3'C. All samples were received intact.
This project was divided into two separate reports due to the different reporting limits for the leachates
and software limitations.
The pH of sample SBR was 7.12 before the extraction procedure began. The sample was leached at a pH
of 4.93, and preserved for storage at a pH of 1.89.
Each sample has been assigned a 9-character !EA lab identification number.
The "E" flag is used on Form I to identify a value· that is estimated due to the presence of an
interference. From the data available, there is no obvious explaination for the "E" flag on barium.
I certify that this data package is in compliance with the terms and conditions of the contract, both
technically and for completeness, for other than the conditions detailed above. Release of the data
contained in this hardcopy data package and in the computer-readable data submitted on diskette has been
authorized by the laboratory manager or his designee, as verified by the following signature.
norganic Data Reviewer
!EA, Inc.
IF.A, Inc Doc# RPF00900.NC
1
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lA CLIENT SAMPLE NC
SW-846 TCLP VOLATILE ORGANICS ANALYSIS DATA SHEET
FP
Lab Name: INDUSTRIAL & ENVIRONMENTAL
Lab Code: IEA
Matrix: Leachate
Sample wt/vol:
Case No.: 619-687 Method: 8240 SDG No.: 03195
Level: (low/med)
% Moisture: not dee.
GC Colurm:DB-624
CAS NO. COMPOUND
5.0 (g/mL) mL
LOW
ID: 0. 53 (mm)
75-01-4----VINYL-CHLORIDE
75-35-4----1,1-DICHLOROETHENE
67-66-3----CHLOROFORM
107-06-2---1,2-DICHLOROETHANE
78-93-3----2-BUTANONE
56-23-5----CARBON TETRACHLORIDE
79-01-6----TRICHLOROETHENE
71-43-2----BENZENE
127-18-4---TETRACHLOROETHENE
108-90-7---CHLOROBENZENE , ,
EPA REGU.
Lab Sample ID: 950319714
Lab File ID:
Date Received:
Date Leached:
Date Analyzed:
0327117.D
03/08/95
03/14/95
03/27/95
Dilution Factor: 1.0
RESULTS:
LEVEL MG/L CRQL MG/L Q
0.20 0.020 0.020
0.70 0.010 0.010
6.0 0.010 0.010
0.50 0.010 0.010
200 0.020 0.020
0.50 0.010 0.010 a.so 0.010 0.010
0.50 0.010 0.010
0.70 0.010 0.010
100 0.010 0.010
022
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05/15/95 15:46 '5'919 677 0427 !EA CARY lill 002/006
lB CLIENT SAMPLE NO. SW-846 TCLP SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
FP Lab Name: INDUSTRIAL & ENVIRONMENTAL
Lab Code: IEA
Matrix: Leachate
Sample •.rt/vol:
case No.: 619-687 Method: 8270 SDG No.: 03195
Level: (low/med)
% Moisture:
500 (g/mL) lnL
LOW
decanted: (Y/N)
Concentrated Extract Volume: 500 (uL)
Injection Volume: 2.0(uL)
GPC Cle~,nup: (Y/N) N pH:
EPA REGU.
Lab Sample ID: 950319714
Lab File ID: 0323605.D
Date Received: 03/08/95
Date Extracted:03/16/95
Date Leached: 03/14/95
Date Analyzed: 03/23/95
Dilution Factor: l.O
CAS NO. COMPOUND LEVEL MG/L CRQL
RESULTS
MG/L Q
106-46-7---1,4-Dichlorobenzene 7.5 0.020 0.020 576-26-1---Total-cresol 200 0.020 0.020 67-72-1----Hexachloroethane 3.0 0.020 0.020 98-95-3----Nitrobenzene 2.0 0.020 0.020 87-68-3----Hexachlorobutadiene 0.5 0.020 0.020 88-06-2·----2, 4, 6-Trichlorophenol 2.0 0.020 0.020 95-95-4·----2, 4, 5-Trichlorophenol 400 0.020 0.020 121-14-:2---2, 4-Dinitrotoluene 0.13 0.020 0.020 118-74-1---Hexachlorobenzene 0.13 0. 020 0. 020 87-86-5·----Pentachlorophenol 100 0.100 0.100 110-86-:L---Pyridine 5.0 0.020 0.020
FORM I SV-1 3/90
027
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lD CLIENT SAMPLE NO.
SW-846 TCLP PESTICIDE ORGANICS ANALYSIS SHEET
FP
Lab Name: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA Case No.: 619-687
Matrix: (soil/water) LEACHATE
Sample wt/vol:
% Moisture:
200 (g/mL) ML
decanted: (Y /N)
Extraction: (SepF/Cont/Sonc) SEPF
Concentrated Extract VolUIDe: lOOOO(uL)
InjectiQn Volume: 1. O (uL)
GPC Cleanup: (Y/N) N pH: --
CAS NO. COMPOUND
58-8 9--9---------gamma-BHC (Lindane)
76-44-8---------Heptachlor
1024-57-3-------Heptachlor epoxiae
72-20-8---------Endrin
72-43-5---------Methoxycnlor
57-74-9---------Chlordane(technical)
8001-35-2-------Toxaphene
FORM I PEST
Method: 8080 SDG No.: 03195
Lab Sample ID: 950319714
Lab File ID: P6032295 011.D
Date Received: 03/08/95
Date Extracted:03/17/95
Date Leached: 03/14/95
Date Analyzed: 03/23/95
Dilution Factor: l.'O
Sulfur Cleanup: (Y/N) N
EPA REGU. RESULTS
LEVEL MG/L CRQL MG/L Q
0.40 0.00025 0.00025
0.0080 0.00025 0.00025
0.0080 0.00025 0.00025
0.020 0.00050 0.00050
10 0.0025 0.0025
0.030 0.0050 0.0050
0.50 0.025 0.025
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Rev 1.0 3/'
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lD CLIENT SAMPLE NO.
SW-846 TCLP HERBICIDE ORGANICS ANALYSIS SHEET
FP
Lab Name: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA Case No.: 619-687 Method: 8150 SDG No.: 03195
Matrix: (soil/water) LEACHATE
Sample wt/vol:
% Moisture:
200 (g/mL) ML
decanted: (Y/N)
Extraction: ( SepF /Cont/ Sonc) SEPF
Concentrated Extract Volume: lOOOO(uL)
Injection Volume: 1. 0 (uL)
GPC Cle,!nup: (Y /N) N pH:
CAS NO. COMPOUND
----------------2,4-D
-----·-----------SILVEX
FORM I HERB
Lab Sample ID: 950319714
Lab File ID: ECD2032595 010
Date Received: 03/08/95
Date Extracted:03/20/95
Date Leached: 03/14/95
Date Analyzed: 03/25/95
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N
EPA REGU. RESULTS
LEVEL MG/L CRQL MG/L Q
10 0.010 0.010
1.0 0.0020 0.0020
u
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Rev 1. o 3/
032
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lB CLIENT SAMPLE NC
SW-846 TCLP SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SBR
Lab Name: INDUSTRIAL & ENVIRONMENTAL
Lab Code: IEA
Matrix: Leachate
Sample ·wt/vol:
Case No.: 619-690 Method: 8270 SDG No.: 03208
Level: (low/med)
% Moist'Jre:
500 (g/mL} mL
LOW
decanted:
Concentrated Extract Volume:
(Y/N)_
500(uL)
Injection Volume: 2.0(uL}
GPC Cleanup: (Y/N) N pH:
EPA REGU.
Lab Sample ID: 950320801
Lab File ID: 0323606.D
Date Received: 03/09/95
Date Extracted:03/16/95
Date Leached: 03/14/95
Date Analyzed: 03/23/95
Dilution Factor: 1.,0
CAS NO. COMPOUND LEVEL MG/L CRQL
RESULTS
MG/L
106-46-7---1,4-Dichlorobenzene 7.5 0.020 0.020
576-26-1---Total-Cresol 200 0.020 0.020
67-72-1----Hexachloroethane 3.0 0.020 0.020
98-95-J----Nitrobenzene 2.0 0.020 0.020
87-68-3----Hexachlorobutadiene 0.5 0.020 0.020
88-06-2----2,4,6-Trichlorophenol 2.0 0.020 0.020
95-95-4----2,4,5-Trichlorophenol 400 0.020 0.020
121-14-2---2,4-Dinitrotoluene 0.13 0.020 0.020
118-74-1---Hexachlorobenzene 0.13 0.020 0.020
87-86-5----Pentachlorophenol 100 0.100 0.100
110-86-1---Pyridine 5.0 0.020 0.020
FORM I SV-1
Q
3/90
009
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CLIENT SAMPLE NO.
SW-846 TCLP PESTICIDE ORGANICS ANALYSIS SHEET
SBR(TCLP)
Lab Name: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Cod.e: IEA Case No.: 619-690
Matrix: (soil/water) LEACHATE
Sample wt/vol:
% Moisture:
200 (g/mL) ML
decanted: (Y/N)_
Extraction: (SepF/Cont/Sonc) SEPF
Concentrated Extract Volume: 10000 (uL)
Injection Volume: 1. 0 (uL)
GPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
58-8 9 ·-9---------gamma-BHC (Lindane)
76-44-8---------Heptachlor
1024-57-3-------Heptachlor epoxiae
72-20-8---------Endrin
7 2 -4 3 ·-5---------Methoxychlor
57-74-9---------Chlordane(technical)
8001-35-2-------Toxaphene
FORM I PEST
Method: 8080 SDG No.: 03208
Lab Sample ID: 95032080l(TCLP)
Lab File ID: P6032295 023.D
Date Received: 03/09/95
Date Extracted:03/17/95
Date Leached: 03/15/95
Date Analyzed: 03/23/95
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N
EPA REGU. RESULTS
LEVEL MG/L CRQL MG/L Q
0.40 0.00025 0.00025 u
0.0080 0.00025 0.00025 u
0.0080 0.00025 0.00025 u
0.020 0.00050 0.00025 u
10 0.0025 0.0025 u
0.030 0.0025 0.0025 u
0.50 0.0050 0.0050 u
Rev 1.0 3/!
014
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CLIENT SAMPLE NO.
SW-846 TCLP HERBICIDE ORGANICS ANALYSIS SHEET
SBR
Lab Name: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Cod,e: IEA Case No.: 619-690 Method,: 8150 SDG No.: 03208
Matrix: (soil/water) LEACHATE
sample wt/vol: 200 (g/mL) ML
% Moisture: ___ decanted: (Y/N) __
Extraction: (SepF /Cont/ Sane) SEPF
Concentrated Extract Volume: lOOOO(uL)
Injecti()n Volume: 1. 0 (uL)
GPC Cleanup: (Y/N) N pH: --
CAS NO. COMPOUND
----------------2,4-D
------·----------SILVEX
FORM I HERB
Lab Sample ID: 950320801
Lab File ID: ECD2032595 012
Date Received: 03/09/95
Date Extracted:03/20/95
Date Leached: 03/15/95
Date Analyzed: 03/25/95
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N
EPA REGU.
LEVELMG/L CRQL
10 0.010
1.0 0.0020
RESULTS
MG/L
0.010
0.0020
Q
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Rev 1.0 3/\
016
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05/15/95 15:46 'a'919 677 0427 !EA CARY @005/006
lB CLIENT SAMl?LE NO SW-S:46 TC!.P SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: INDUSTRIAL & ENVIRONMENTAL FPSPK
Lab Cede: IEA
Matrix: Leachate
Sample wt/vol:
case No.: 619-687 Method: 8270 SDG No.: 03195
Level: (low/med)
% Moisture:
500 (g/mL) mL
LOW
decanted:
Concentrated Extract Volume:
(Y/N)
500(uL)
Injection Vol1lllle: 2.0(uL)
GPC Cl<~anup: (Y/N) N pH:
EPA REGU.
Lab Sample ID: 950319714SPK
Lab File ID: 0323607.D
Date Received: 03/08/95
Date Extracted:03/16/95
Date Leached: 03/14/95
Date Analyzed: 03/23/95
Dilution Factor: 1.0
CAS NO. COMPOUND LEVEL MG/L CRQL
RESULTS
MG/L. Q
106-46-7---1,4-Dichlorobenzene 7.5 o. 020 0.035 576-26-1---Total-Cresol 200 0.020 0.003 67-72-·l----Hexachloroethane 3.0 0.020 0.034 98-95-·3----Nitrobenzene 2.0 0. 020 0.020 87-68-·3----Hexachlorobutadiene 0.5 0.020 0.037 88-06-·2----2, 4, 6-Trichlorophenol 2.0 0.020 0.002 95-95-4----2,4,5-Trichlorophenol 400 0.020 0.002 121-14-2---2,4-Dinitrotoluene 0.13 0.020 0.020 118-74-1---Hexachlorobenzene 0.13 0.020 0.032 87-86-5----Pentachlorophenol 100 0.100 0.003 110-86-1---Pyridine 5.0 0.020 0.029
FORM I sv-1 3/90
J
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lB CLIENT SAMPLE NC
SW-846 TCLP SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TCLP239
Lab Name: INDUSTRIAL & ENVIRONMENTAL
Lab Code: IEA
Matrix:: Leachate
Sample wt/vol:
Case No.: 619-690 Method: 8270 SDG No.: 03208
Level: (low/med)
% Moisture:
500 (g/mL) mL
LOW
decanted: (Y/N)
Concentrated Extract Volume: 500 (uL)
Injection Volume: 2.0(uL)
GPC Cle,anup: (Y/N) N pH:
EPA REGU.
Lab Sample ID: TCLP239
Lab File ID: 0322612.D
Date Received: / /
Date Extracted:03/16/95
Date Leached: 03/14/95
Date Analyzed: 03/22/95
Dilution Factor: 1.0
CAS NO. COMPOUND LEVEL MG/L CRQL
RESULTS
MG/L
106-46-7---1,4-Dichlorobenzene 7.5 0.020 0.020
576-26-1---Total-Cresol 200 0.020 0.020
67-72-1----Hexachloroethane 3.0 0.020 0.020
98-95-3----Nitrobenzene 2.0 0.020 0.020
87-68-3----Hexachlorobutadiene 0.5 0.020 0. 020
88-06-2----2,4,6-Trichlorophenol 2.0 0.020 0.020
95-95-4----2,4,5-Trichlorophenol 400 0.020 0.020
121-14-2---2,4-Dinitrotoluene 0.13 0.020 0.020
118-74-1---Hexachlorobenzene 0.13 0.020 0.020
87-86-5----Pentachlorophenol 100 0.100 0.100
110-86-1---Pyridine 5.0 0.020 0.020
FORM I SV-1
Q
3/90
010
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lB CLIENT SAMPLE NC
SW-846 TCLP SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SVB258
Lab NaI-le: INDUSTRIAL & ENVIRONMENTAL
Lab Code: IEA
Matrix: Water
Sample wt/vol:
Case No.: 619-690 Method: 8270 SDG No.: 03208
Level: (low/med)
% Moisture:
1000 (g/mL) mL
LOW
decanted:
Concentrated Extract Volume:
(Y/N)_
lOOO(uL)
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH:
EPA REGU.
Lab Sample ID: SVB258
Lab File ID:
Date Received:
0322604.D
I I
Date Extracted:03/16/95
Date Leached: / /
Date Analyzed: 03/22/95
Dilution Factor: 1.0
.CAS NO. COMPOUND LEVEL MG/L CRQL
RESULTS
MG/L Q
106-46-7---1,4-Dichlorobenzene 7.5 0.020 0.020
576-26-1---Total-Cresol 200 0.020 0.020
67-72-1----Hexachloroethane 3.0 0.020 0.020
98-95-3----Nitrobenzene 2.0 0.020 0.020
87-68-3----Hexachlorobutadiene 0.5 0.020 0.020
88-06-2----2,4,6-Trichlorophenol 2.0 0.020 0. 020
95-95-4----2,4,5-Trichlorophenol 400 0.020 0.020
121-14-2---2,4-Dinitrotoluene 0.13 0.020 0.020
118-7 4·-1---Hexachlorobenzene 0.13 0.020 0.020
87-86-5----Pentachlorophenol 100 0.100 0.100
110-86-1---Pyridine 5.0 0.020 0.020
FORM I SV-1 3/90
034
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u u u u
4B I
I
SW-846 SEMIVOLATILE METHOD BLANK SUMMARY
Lab Name: INDUSTRIAL & ENVIRONMENTA
Lab Code: IEA Case No.: 619-690 I Lab File ID: 0322612 .D
Instrument ID: MSD6
Matrix:: Leachate
Method:
Lab
Date
Date
Time
CLIENT SAMPLE NO.
TCLP239
8270 SDG No. : 03208
Sample ID: TCLP239
Extracted: 03/16/95
Analyzed: 03/22/95
Analyzed: 1903
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i?HIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
.27
28
29
30
COMMENTS:
I CLIENT
SAMPLE NO.
====----------
SBR
page 01 of 01
LAB LAB DA'l'.i,;
SAMPLE ID FILE ID ANALYZED ============== -----=======-= ==========
950320801 0323606.D 03/23/95
FORM IV SV 3/90
030
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CLIENT SAMPLE NO.
SW-846 TCLP PESTICIDE ORGANICS ANALYSIS SHEET
TCLP239
Lab Name: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA Case No.: 619-690
Matrix: (soil/water) LEACHATE
Sample wt/vol:
% Moisture:
200 (g/mL) ML
decanted: (Y/N)_
Extraction: (SepF/Cont/Sonc) SEPF
Concentrated Extract Volume: 10000 (uL)
Injection Volume: 1. 0 (UL)
GPC Cleanup: (Y/N) N pH: --
CAS NO. COMPOUND
58-89-9---------gamma-BHC (Lindane)
76-44-8---------Heptachlor
1024-57-3-------Heptachlor epoxiae
72-20-8---------Endrin
72-43-5---------Methoxychlor
57-74-9---------Chlordane(technical)
8001-35-2-------Toxaphene
FORM I PEST
Method: 8080 SDG No.: 03208
Lab Sample ID: TCLP239
Lab File ID: P6032295 003.D
Date Received: / /
Date Extracted:03/17/95
Date Leached: 03/15/95
Date Analyzed: 03/22/95
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N
EPA REGU. RESULTS
LEVEL MG/L CRQL MG/L Q
0.40 0.00025 0.00025 u
0.0080 0.00025 0.00025 u
0.0080 0.00025 0.00025 u
0.020 0.00050 0.00025 u
10 0.0025 0.0025 u
0.030 0.0025 0.0025 u
0.50 0.0050 0.0050 u
Rev 1. O 3/:
015
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CLIENT SAMPLE NO.
SW-846 TCLP PESTICIDE ORGANICS ANALYSIS SHEET
TCLP238
Lab Na:me: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA Case No.: 619-687
Matrix: (soil/water) LEACHATE
Sample wt/vol:
% Moisture:
200 (g/mL) ML
decanted: (Y/N)
Extraction: (SepF/Cont/Sonc) SEPF
Concentrated Extract Volume: 10000 (UL)
Injection Volume: 1. 0 (UL)
GPC Cleanup: (Y/N) N pH: --
CAS NO. COMPOUND
58-89-9---------gamma-BHC (Lindane)
76-44-8---------Heptachlor
1024-57-3-------Heptachlor epoxiae
72-20-8---------Endrin
7 2-4 :;. -5---------Methoxychlor
57-74-9---------Chlordane(technical)
8001-35-2-------Toxaphene
FORM I PEST
Method: 8080 SDG No.: 03195
Lab Sample ID: TCLP238
Lab File ID: P4032195 023.D
Date Received: / /
Date Extracted:03/17/95
Date Leached: 03/14/95
Date Analyzed: 03/22/95
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N
EPA REGU. RESULTS
LEVEL MG/L CRQL MG/L Q
0.40 0.00025 0.00025
0.0080 0.00025 0.00025
0.0080 0.00025 0.00025
0.020 0.00050 0.00050
10 0.0025 0.0025
0.030 0.0050 0.0050 a.so 0.025 0.025
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Rev 1. o 3/
030
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4C CLIENT SAMPLE NO.
SW-846 PESTICIDE METHOD BLANK SUMMARY
TCLP239
Lab Name: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA Case No.: 619-690 Method: 8080 SDG No.: 03208
Lab File ID: P6032295 003 Lab Sample ID: TCLP239
Matrix: (soil/water) LEACHATE
Sulfur Cleanup: (Y/N) N
Extraction: (SepF,Cont/Sonc) SEPF
Date Analyzed (1): 03/22/95
Time Analyzed (1): 1921
Instrument ID (1): HP5890P6
GC Column (1) :RTX-35 ID: 0.53(mm)
Date Extracted: 03/17/95
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD
COMMENTS:
page 01 of 01
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
CLIENT
SAMPLE NO.
--=========-
SBR(TCLP)
SBRSPK
LAB
SAMPLE ID
==============
950320801(TCLP
950320801SPK
FORM IV PEST
DATE TIM.i:;
ANALYZED ANALYZED
------------========
03/23/95 1537
03/23/95 1643
039
3/90
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CLIENT SAMPLE NO.
SW-846 TCLP HERBICIDE ORGANICS ANALYSIS SHEET
TCLP239
Lab Name: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA case No.: 619-690
Matrix: (soil/water) LEACHATE
Sample wt/vol:
% Moisture:
200 (g/mL) ML
decanted: (Y /N)
Extraction: (SepF /Cont/Sonc) SEPF
concentrated Extract Volume: lOOOO(uL)
Injection Volume: 1. 0 (uL)
GPC c1,2anup: (Y/N) N pH: --
CAS NO. COMPOUND
----------------2,4-D
----·------------SILVEX
FORM I HERB
Method: 8150 SDG No.: 03208
Lab Sample ID: TCLP239
Lab File ID: ECD2032595 006
Date Received: / /
Date Extracted:03/20/95
Date Leached: 03/15/95
Date Analyzed: 03/25/95
Dilution Factor: 1,0
Sulfur Cleanup: (Y/N) N
EPA REGU. RESULTS
LEVEL MG/L CRQL MG/L Q
10 0.010 0.010
1.0 0.0020 0.0020
u u
Rev 1. O 3/
017
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CLIENT SAMPLE NO.
SW-846 TCLP HERBICIDE ORGANICS ANALYSIS SHEET
TCLP238
Lab Name: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA Case No.: 619-687 Method: 8150 SDG No.: 03195
Matrix: (soil/water) LEACHATE
Sample wt/vol:
% Moisture:
200 (g/mL) ML
decanted: (Y/N)
Extraction: ( SepF /Cont/ Sane) SEPF
concentrated Extract Volume: lOOOO(uL)
Injection Volume: 1. 0 (UL)
GPC Cleanup: (Y /N) N pH:
CAS NO. COMPOUND
----------------2,4-D
----------------SILVEX
FORM I HERB
Lab Sample ID: TCLP238
Lab File ID: ECD2032595 005
Date Received: / /
Date Extracted:03/20/95
Date Leached: 03/14/95
Date Analyzed: 03/25/95
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N
EPA REGU. RESULTS
LEVEL MG/L CRQL MG/L
10 0.010 0.010
1.0 0.0020 0.0020
Q
u u
Rev 1.0 3/'.
033
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CLIENT SAMPLE NO.
SW-846 TCLP HERBICIDE ORGANICS ANALYSIS SHEET
SBRSPK
Lab li'ame: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA Case No.: 619-690 Method: 8150 SDG No.: 03208
Matrix: (soil/water) LEACHATE
Sample wt/vol:
% ·Moisture:
200 (g/mL) ML
decanted: (Y/N)
Extraction: (SepF/Cont/Sonc) SEPF
concentrated Extract Volume: lOOOO(uL)
Injection Volume: 1. 0 (uL)
GPC Cleanup: (Y /N) N pH: --
Lab Sample ID: 950320801SPK
Lab File ID: ECD2032595 013
Date Received: 03/09/95
Date Extracted:03/20/95
Date Leached: 03/15/95
Date Analyzed: 03/25/95
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N
EPA REGU. RESULTS
CAS NO. ·COMPOUND LEVEL MG/L CRQL MG/L Q
----------------2,4-D ---·-------------SILVE..,X __________ _ 1 i~o I
0.0101 0.0561 0.0020 0.010
FORM I HERB Rev 1.0 3/~
048
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4C CLIENT SAMPLE NO.
SW-846 HERBICIDE METHOD BLANK SUMMARY
TCLP239
Lab Name: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA case No.: 619-690 Method: 8150 SDG No.: 03208
Lab Sample ID: TCLP239
Matrix: ( soil/water) LEACHATE
sulfur Cleanup: (Y/N) N
Date Analyzed (1): 03/25/95
Time Analyzed (1): 1327
Instrument ID (1): ECD2
Lab File ID: ECD2032595 006
Extraction: (SepF,Cont/Sonc) SEPF
Date Extracted: 03/20/95
GC CCllumn (l):RTX-35 ID: 0.53(mm)
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD
COMMENTS:
page 01 of 01
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
CLIELu
SAMPLE NO.
============
SER
SBRSPK
LAB
SAMPLE ID ==============
950320801
950320801SPK
FORM IV HERB
uATi:; Tl.ME
ANALYZED ANALYZED ==========
03/25/95 1548
03/25/95 1612
Rev 1.1 3/9·
04 6
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lH CLIENT SAMPLE NO.
SW-846 HERBICIDE ANALYSIS DATA SHEET
HB495
Lab N'ame: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA Case No.: 619-690
Matrix: (soil/water) WATER
Sample wt/vol:
% Moisture:
1000 (g/mL) ML
decanted: (Y/N)
Extraction: (SepF/Cont/Sonc) SEPF
Concentrated Extract Volume: 10000 (uL)
Injection Volume: 1. 0 (uL)
CAS NO. COMPOUND
----------------2,4-D
--------~-------SILVEX
----------------2,4,5-T ACID
Method: 8150 SDG No.: 03208
Lab Sample ID: HB495
Lab File ID: ECD2032595 004
Date Received: / /
Date Extracted:03/20/95
Date Analyzed: 03/25/95
Dilution Factor: 1.0
CONCENTRATION UNITS:
(mg/Lor mg/KMG/L
0.0020
0.00040
0.0030
Q
u u u
FORM I HERB Rev 1.1 3/93
045
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lH CLIENT SAMPLE NO.
SW-846 HERBICIDE ANALYSIS DATA SHEET
HIBLKAA
Lab Name: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA case No.: 619-690
Matrix: (soil/water) WATER
Sample wt/vol: (g/rnL) -
% Moisture: decanted: (Y/N)
Extraction: (SepF/Cont/Sonc)
Conc,~ntrated Extract Volume: ___ (uL)
Inje,;tion Volume: 1. 0 (UL)
CAS NO. COMPOUND
----------------2,4-D
----------------SILVEX
----------------2,4,5-T ACID
Method: 8150 SDG No.: 03208
Lab Sample ID: HIBLKAA
Lab File ID: ECD2032595 001
Date Received:
Date Extracted: ___ _
Date Analyzed: 03/25/95
Dilution Factor: 1.0
CONCENTRATION UNITS:
(mg/Lor mg/KMG/L Q
0.0020
0.00040
0.0030
u u
u
FORM I HERB Rev 1.1 3/93
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4C CLIENT SAMPLE NO.
SW-846 HERBICIDE METHOD BLANK SUMMARY
HB495
Lab Name: INDUSTRIAL & ENVIRONMENTAL ANALYSTS
Lab Code: IEA Case No.: 619-690 Method: 8150 SDG No.: 03208
Lab Sample ID: HB495
Matrix: (soil/water) WATER
Sulfur Cleanup: (Y/N) N
Date Analyzed (1): 03/25/95
Time Analyzed (1): 1241
Instrument ID (1): ECD2
Lab File ID: ECD2032595 004
Extraction: (SepF,Cont/Sonc) SEPF
Date Extracted: 03/20/95
GC C::>lumn (1) :RTX-35 ID: 0.53(mm)
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD
COMMENTS:
page 01 of 01
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CL.LENT
SAMPLE NO.
-======-====
SBR
TCLP239
SBRSPK
LAB DATE TIME
SAMPLE ID ANALYZED ANALYZED
======--===----=========
950320801 03/25/95 1548
TCLP239 03/25/95 1327
950320801SPK 03/25/95 1612
FORM IV HERB Rev 1.1 3/9
044
I~--IEA ~:-U An"4J;ari0nCompany
I
Report Date:
Cl:lent:
Prc)ject:
03/20/95
IEA
619-687S
IEA
Sampl.e
# Client ID
IEA LABORATORY RESULTS
Parameter Results
Received Date: 03/10/95
IEA Job Number: 0020-446
Units PQL
Dat:e
Analyzed
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•m•:••••••••••••••-••••••••••••••••••••••=•••••11:1•••••••••c===••=D•111••••••••••a••••••••
l IT EFFL
2 INT INFL
Met:hod Blank
20-<148-l/MS
20-<.48-1/MSD
COMMENT~;:
Ethylene glycol
Et.hylene glycol
Ethylene glycol
Et.hylene glycol
Ethylene glycol
PQL. Practical Quantitation Limit
BQL. Below Quantitation Limit
Analyzed by direct injection GC-FID
By: LSB
MS/MSD RPD • 14
Result3.wkl Rev. 041393
BQL
1,800
BQL
60
69
mg/L
mg/L
mg/L
t
t
10 c' 03/18/95
250 03'/18/95
10 03/18/95
03/18/95
03/18/95
057
~ cw,~~
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Report Date:
Client:
Project:
03/20/95
IEA
619-687S
IEA
Sample
# Client ID
IEA LABORATORY RESULTS
Parameter Results
Received Date:
IEA Job Number:
Units
03/14/95
0020-448
PQL
Date
Analyze:'
======================================================================================:
l V-23
Method Blank
··1/MS
Ethylene glycol
Ethylene glycol
Ethylene glycol
Ethylene glycol ··1/MSD
COMMENTS:
PQL = Practical Quantitation Limit
BQL = Below Quantitation Limit
Analyzed by direct injection GC-FID
By: LSB
MS/MSD RPD = 14
Result3.wkl Rev. 041393
2,900
BQL
60
69
mg/L
mg/L
500 ·
10
\. .
03/18/9:
-03./18/9:
03/18/9:
03/18/9:'
058
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