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HomeMy WebLinkAboutNCD000813592_19970113_GA-Pacific Corp Hdwd Saw_SERB PA SI_Expanded Site Inspection - Volume II-OCR-- - - --- - -- -r - I I I I I I I I I I I I I I I I I I I REF. 2 LATITUDE AND LONGITUDE CALCULATION l.;QR}',SHE:ET 12 LI USING ENGINEER'S SCALE (1/60) AK.A: SSID: --------------------------------·----- ADDRESS: __ __,p'-'-,/,,..t-'--""-~..c."_d __ T::>_,_;_..,_e. _______________________ _ CITY: ----'-c-,;,l,_i ,.__Y_~_"_..,_f'_i,, ______ _ ZIP CODE: 2 7962 STATE: __ N_L-__ _ ---------- SI TE REFER.EN CE PO I NT: --"lt~p:LP:c•..:;•_.,:<.'-';'-',.,'--'-=-· Lk.:,_,_,,cl_;;<><:,_•:.:·•:..:./,..:.'.:.;,:..:~ __ ,_.,_,c __ 'l>-'.J, f,'----'.T...:-="-'---'ic'--------- '?1 ~·.., ft. ~ USGS QUAD HAP NA.ME: Cc".._5f TOW1"/ SH 1 P: N/S RANGE: E/W ' SCALE: 1:24,000 HAP DATE: 197<-/ SECTION: 1/4 1/4 ---1/4 HAP DATUH: @5) 1983 (CIRCLE Ot!E I HE RID IAN: COORDINATES FROM LOWER RIGHT (SOUTHEAST) CO;\NER OF 7.5' HAP (attach phot:ocopy): LONGITUDE: 7 (, o 37 ' 3o " LATITUDE: '35 ° l/5' 0,, COORDINATES FROH LOWER RIGHT (SOUTHEAST) CORNER OF 2.5' GRID CELL: LONGITUDE: ~o 1/)' )C,,, LATITUDE: 5o, 0 ,, CALCULATIONS: LATITUDE (7.5' QUADRANGLE ~J\P) A) NUMBER OF RULER GRADUATIONS FROM LATITUDE GRID LINE TO SITE RI:F POINT: li45 8) MULTIPLY (A) BY 0,3304 TO CONVERT TO SECONDS: Ax 0.3304 i'11. ()3 ,, ---- C) EXPRESS IN HIHUTES AHO SECONDS ( l '= 60" I: v , -1:__• '2-7 . D3 " D) ADD TO STARTING LATITUDE: + '2-, 27 0 ------ SITE LATITUDE: '35 o 5')..., "27. 0 " CALCULATIONS: LONGITUDE (7.5' QUADRANGLE HAP) A) NUMBER OF RULER GRADUATIONS FROM RIGHT LOtlGITUDE LINE TO SITE REF POINT: ·3-5._', B) t!ULTI?LY (A} BY 0.3304 TO COh'VERT TO SECOh'DS: Ax 0.3304 l I l , 3 · C) EZ?RESS IN HINUTES AND SECONDS (l'= 60"): I , 57 -~ ,, D) ADD TO STi-.RTING LOtlGITUDE: i , 57 . "3 INVESTIGATO?.: __ _,c"'-'· 'c._t:,,_._Q_, _.,_,,.,.,_r:o __ r_c_l ________ _ DATE: E-10 I , ·C - ¥• ~--" I:, NUHBER: rJlD CCO g1:; S?2 I I I I I I I I I I I I TOPOGRAPHIC MAP QUADRANGLE NA~IE: ___ ?_· _l_,fc...,_"_v_f_l.. __ E_c_,_>_·f-_________ SCALE: 1:2'.CXJO COORDINATES OF LOWER RIGHT-HA.~D CORNER OF 2.5-MINUTE GRJD: I LATITUDE: '35o 5'0' _Q___· LONGITUDE: lf•o 'fl· 3.:, · E-11 I I I TECHNICAL PAPEH NO. 110 HAINFALL FHEQUENCY A'l'LAS or 'l'IIE llNl'l'EI) S'l'A'l'ES fnr Durations fro111 30 Mi1111lc3 lo 2,(. I lou·rs a11d flelur11 Periods f1·0111 I lo ] 00 Y1'.a1·s IIA\ IIJ M. JU:H!'-IIHt-:1.U \ PRCPERTY OF EPA FITIV Cl Georgia-Pacific Corp. Hardwood Sa\wnill NCD 000 813 592 Commerce l'.761 Technical Pn er 11nrr:r:rnr Ref. 4 ,_ "y ~l ~ --~ ·. --, . /4: '<·:':- ~~: , m• ~- --lri'Pm'i ~· ( .,. ··-.:· . .. '. ' Environmental Science S.ervice5 Administration Environmental Data Service -----l------j-----1-----1-----1------ o· -----1-----1-----1-----r-----1-----_, -----1-----1--~--~-1-----1------1----- -----1-----------1-----1---- n -i---rf--r'--r---i--'-n"n---+-,'.-4-~~;-.;:'-,-~~~~-/~2~~~19'..;~ £,.' u--7-t-t-t-t--t-t-=i=,:_ -(_ ':.:S l-l-l--l---l--1-1-1-l-j: ----- -, ---f-i""R"'Pf-f---1 ffr== ~i~ :l:t; ~ = !.. ~ • , 11:J [ §e i,; ,+..,Ll I" <--, "'i-C ---'-~ _ _s __ S.==·,:.:_j~ ----J =)1r=~1:f-.~t:~,.,l ::ti 'Iii' • .,, I • N ,, S!t!Ul"" H--+---0';'-~:r--. J-~ ];I 1-1---l--H------ - - -__ Jc &,:1_ J__,__ Ed ___ ✓,, -_' -~}".:::::: -"".!. ~---,- --Jq ---'-/~-''....::> -';J,; ; _, r_r1 f to __ • __ ,/., • =C -~-.c1--~-~ _--ri--i-~i k=•-,---J ,i_ ----f'-f --~--------i ~-_:__ _ l) __ f Pf o ,,..,_ __ c:-i _ _ __ _ _ 1..-, _________ cl •- HH-1--1----- --,-1--1-1-J -----,_ -·--1------- -------1--- ·--------- ------1--1- -------·-1-- ·1 ' . '*~t"Si' ;ff~:' "~~:_ -/~-- ' ',• . '· -~ ' ' ·- ,i ,, ~ .,. . ' '}; :rt ., ' ,. •, (.1;. ~~; ~~-·--fi· ,.~1,.~~A~· I I I I I I I I I I I I I I I I I I I Site Name: Site Number: Site Location: Date: . Distance from Site Location 0 to 1/4 mile > I /4 to 1/2 mile > 1/2 to I mile >I to 2 miles >2 to 3 miles >3 to 4 miles REF. 6 GA-Pacific Corp. Hardwood NCO 000 813 592 Plymouth, N.C. Washington County Latitude: 35 52 27.0 Longitude: 76 44 27.5 March 29, 1995 Calculation Results Population Number of Households Per Ring Cumulative Per Ring Cumulative 92 92 42 42 478 570 176 218 1,357 1,927 527 745 2,603 4,530 998 1,743 1,354 5,884 501 2,244 I, 118 7,002 424 2,668 Note: . The populations and number of households within specified target distance rings were calculated for the NC Superfund Section by the NC State Center for Geographic Information and Analysis using the 1990 US Census data. These values were calculated by summing the population and the number of households data for each census block located within each target ring. For census blocks lying only partially within the ring, the per cent area of the block within the ring was multiplied by the population and household densities of the block. I 0 I I I I I I I I I I I I I I 1. REF. 7 RCRA INSPECTION REPORT Facility Information Georgia Pacific Corporation HDWD Sawrni 11 Plywood Drive Plymouth, NC Washington County NCD000813592 2. Facility Contact Gerald Tice, Environmental Engineer 3. Survey Participant Fred Wood, District Sanitarian, DHS 4. Date of Inspection October 21-, 1981 5. Applicable Regulations 40 CFR Part 262 and 265 May 19, 1980. 6. Purpose of Survey RCRA Status Inspection including review of records, site survey and sampling procedures. Regulatory requirements covered included those contained in 40 CFR Par't 262 and 265. 7. Facility Description The Georgia Pacific Corp. sawmill is located on 25 acres of land on Plywood Drive in Plymouth. This property is bordered by the Roanoke River. This facility produces hardwood lumber, railroad ties, etc. According to Mr. Gerald Tice this plant has a NPDES permit from NRCD that was inadvertently left off the Part A application. The waste produced at this plant consists of waste oil, solvents, wood treatment chemicals, and pesticides. These chemicals are used as a wood fungicide and insecticide. They are manufactured by Coppers Co. of St. Louis, Missouri under the trade.name Noxtane. Noxtane contains pentachloropheneate and sodium metaborate and other chlorophenols. The insecticide contains lindane. The chemical waste is the result of dripping on the ground after the wood passes through the dip vat. Most of this waste occurs at the end of the conveyor system. I got conflicting information on where the waste is disposed. One person said it was cleaned up and burned in the boilers and another said it was carried to the county landfill. (,1~-;;... i:c.,:_..ef';) ----.·-·,. Mr. Tice left instructions that from now on all waste material from this area will be put in drums and stored in the hazardous waste storage area. ,.//., //:{fl ~ -d 6-t 4£.J-f, ) r H ..,, -f ,~v"r - t I I I I I I I I I I I I I I I I I - 2 - 8. Documentation of Site Deficiencies 9. Georgia Pacific Corp. HDWD Sawmill was deficient in the following areas: 1. Not providing a waste analysis plan. (265.13) 2. Inspection Requirements. (265.15) 3. Personnel Training Records. ( 265.16) 4. Arrangements with local authorities. (265.37) 5. No contingency plan. (265.50 -265.56) 6. No closure plan. (265.111-265.115) 7. Financial Requirements. (265.142) Recommendations It is recommended the facility take immediate action in complying with the above deficiencies. ·lo. Compliance Schedule All above deficiencies must be corrected on or before January 1, 19P2. ii II II p II· j1 p I' ti II , fl ,,. REFERENCE N REF. 8 l!lil Georgia-Rlcific Corporation E.a.rurn Wood Prod:tm . January 28, 1985 Ms, Lee Crosby, Chemist North Carolina Division of Health Services P. 0, Box 2091 Raleigh, North Carolina 27602-2091 Re: ERRIS Listing Dear Ms. Crosby: Manufacturing Division P.O. Box 105603 Atlanta, Gtorgia 30348 Ttl,pbon, (404/ 521-4000 T,!,ryp, (8101 751-1000 As per your Decemb~r 4, 1984 letter, the following is the requested information ~hich pertains to our plant locations included on the ERRIS listing~ .. 1. Enfield (NCD000773507) hardwood sawmill Location -S, Dennis Street Ext.)off U.S. 301 S),. Enfield, North Carolina Start-up of manufacturing operations -1977 2. Bowdens (NCD000773515) hardwood sawmill Location -off Secondary Rt. 1301, Bowdens, North Carolina Start-up ~f manufacturing operations -1980 3. Plymouth-(NCD000813592).hardwood sawmill. Location -Plywood Dr., .. :. Plymouth, North Carolina Start-up of manufacturing operations This facility was purchased from Atlas Plywood around 1950. The purchased structure was theri torn down and a new facility constructed.· Becatise of a fire in 1983 this plant was permanently closed. 4. Conway (NCD044388015) hardboard facility Location -County Rd. 35, Conway, Noith Carolina Start-up of maufacturing operations -1960 Site Monitoring Of the four facilities, only the Conway hardboard plant has groundwater monitoring wells located on its plant site. These wells were installed primarily because the plant site storm . It Zl!45f Jt, 1 .. LZ .Ui!1JE,fi)1 WWWW,12 J!A€&M!tb,QJ;&&™~J&L- 11 :··-· .. ·1· ii ii p 11 P. p· fl Page Two Ms. Lee Crosby January 28, 1985 run-off at the adjacent Georgia-Pacific Resin facility and run-off from material storage areas at the hardboard plant are collected and treated in an aerated lagoon system. The ~ffluent from the lagoon is spray irrigated (N.C. Permit #6376-R) on ~he hardboard plant's property. The collection of well samples and submittal of monthly monitoring reports is performed by the resin plant. A sketch of the well locations is attached. Past Waste Handling Practices Based on current and past knowledge of the fo~r manufacturing operations we do not suspect that any toxic or hazardous. materials were buried on or off the plant sites. We make this statement knowing that the process operations for.these plants has remained virtually unchanged over the years. Plant Site Drawings A si.te plan for each of the subject facilities is enclosed. We trust this provides the n~essary data for completion of your survey. If further _discussio~ is required; please conta~t my office at 404-521-5080. Very truly yours, p . . -/2~ 5~~~ . . . . . P ~ TO; B. STEVENS · . · . · • ·---: ENVIRONMENTAL ENGINEER . . . EASTERN WOOD.PRODUCTS MANUFACTURING DIVISION TBS:gr Attachment/Enclosures cc: Messrs: A. T. Johnson G. W. Tice G. F. McCaig • Please print (!r type in the unshaded areas only REF.9 .. -Form Approved 0MB No. 158-R0175 . rm: -in .?~eas are spaced far elite type, i.e., 12 characters/' -··'10).'-----• ---, . ,PA 1.D. NUMBER .Fo:::M :.... u.s. EN. .>N.MENTAL pf, GEJRAL &EPA Gt:l'JERAL INFORMATION FNCD000813592 · ·· · Consolidated Permits Program (Read the "General In,tru.ctions'" before .tarting.) 11 ,. t GENERAL INSTRUCTIONS ff a preprinted label has; been provided, aff · it::ln the designated space. Review the inforr ation carefully; if any of it is incorrect, ere through it and enter the correct data in. ti appropriate fill-in area below. Also, if'any , the preprinted data is absent (the·area to ti left of· the label· spBCe lisu the infarmatic that should appear). please provide it in t: proper fill:....in area(s) 1 below. If the label complete and correct; you need not comple . Items I; ,Ill, V, and VI (except Vl·B whit must be completed regardless). Complete : items it. no label has been· provided. Refer · , the instructions· for detailed· item· descri ·tions· and for· the• legBI authorizations unC which this data is collected .. · · ·· · ·•·: · 'INSTRUCTIONS:; Complete 'A through J to determine;whether. you need to submit any permit application forms to the EPA..lf you answer."yes'.' to.any questions, you must submit this.form· and the supplemental form listed in:the .parenthesis following the question. Mark "X" in the box in the third column if the suppleme·ntal:form is 'attached •. If. you answer "no'.'. to 'each question, you need not submit any of these forms.You may answer, "no" if youcac!(vity is excluded frorri'pe!11lit requirementt; see Section C of the instructions. See also, Section D of the instructions for definitions of bold-fec,,d terms.·,· ·· YCI, .NO 1"0"'M ATTAC:MC A.::-1 s; · 'th iS'.~ ·fa~i lit'v, :'8? publicly ::·'Clwned ':treatment:·. works \Which {'ri:sUlts :ifl'.:a:,,disch8rge :to (waters of the· U.S;?. 'F,OR.~.: 2~l ,.\ffi~J~. ->i?'~.;~t~\Y:t,_~~\)?{<:: ;.::, _; ;;·\·:.:·;. ~1--+cx~,.,,,+-.,.,.,---j ls,t is~a. acility-w 1c "currently resu ts· in tse arges to watari of.,tha:U,S;.'other. than those described in A or B abo\le? FORM 2C o you·or w1 you·iniect at t 1s acz 1tv any pro uc water.Or·otherrfluids whic:h1.are brought to the surface in connection· with conventional oil or natural gas pro- . -duction;' inject· fluids used for enhanced recovery of ·,.~··:-~oil or·natural gas;:or•iriject~fluids,for. storage of liquid _..,, .. h drOcarbons? {FORM"4). ;:~,-• · ... :, ... ~• ., .... ·· .... , s t is-. ac1 tty a proposed stationary source wnicn 1s one·· oF the· 28.-industrial categories, listed in the in- structions and•,which will, potentially emit 100 tons X " X per year.· oF=8nv.'.Sir· pollutant regulated under the . Clean Air Act: arid "1ay :affect. or be located in en attainment area? (FORM'S) ,•• 1-~1-.,--1~-~--1 Ill. NAME CF FACILITY· A. STREET OR P.O. BOX 0 B O X 1 8 0 8 B. CITY OR TOWN SPECIP'IC QUESTIONS B;. Does or will·this facility (either existing or proposed)•. Include a concentrated· animal feeding operation· or aquatic-'animal· production facility which· results in, a, .. dis::herge to waten of the U.S.7 (FORM 28) . , . ! ·:~. D. Is this a propo aciilty o er than those described . in A ors· above)"which will result in a discharge.to~ waters of the U.S.? !FORM 201 F. Do you or will you inject at this facility industrial or municipal effluent below the lowermost stratum con- taining; •within one quarter mile· of• the well bore, underground sources of drinking water? (FORM 4) 1 H. Do you or will you inject at this facility fluids toi spe- cial processes such as mining of·sulfur by the Frasch· process, solution mining of minerals, in situ· comb'us-· tion of fossil, fuel, or recovery of geothermal. energy? IFORM 4) . ' ·.:,::-_ :;;c:' •f:, .' J. Is this ac1lity a propos stationary source wh1cn 1s NOT one of the 28 industrial categories listed in the instructions and which will potentially emit 250 tons ,, M X •·• ll X .• l7 X " X . ,. X per year of any air pollutant regulated under the Clean Air Act and may affect or be located in an attainment· a,..1 I FORM 51 l-c4~+-~ e. PHONE (area code & no.) 4 0 4 7 1 5 1 A. STREET, ROUTE.NO. OR OTHER SPECIFIC IOENT1FIER W O O D D R I V E B. COUNTY NAME SHINGTON " C. CITY. OR TOWN'. H .. O.STATE E. ZIP COOE 2 7 9 6 2 F. COUNTY COO · n n . ,. COl1TINUE ON REVE SIC CODES (4-digir, in order of prioriry; ·' A, FIRST (specify J 4 2 1 Pl r M. 7 7 C. THIRO D. FOURTH (specify/ . OPERATOR INFORMATION A. NAME B. l:1 the neme listed In 1-,:;:::-,--,--,--,--,--,--,--,--,--,--,--,-,--,---,-,--,--,-,--,-,-,---,-,-,--,--,,-,-,,-,-,-,-,T,-r,,---j Item V 11 l·A alao the owner? E O R G I A -P A C I F I C C O R P O R A T I O N -A U G U S T A GA ~ YES ONO •• .. c. STATUS OF OPERATOR (Enter the appropriate lerter into the answer box; if "Other", specify.) D, PHONE (area code & no.) 7 1 5 1 " " ; ,•·:c'E. STREET OR P.O. BOX 0 B O X 1 8 0 8 · F:·clTY OR TOWN IX. INDIAN LAND U G U S T A ts the facility located on Indian lands?..,. ' . ·' .,, • V'"· 0 YES [],NO:. . . ·,s,•:c !12 •. ••. :_."},?.;;:~. A. NPOES (Discharges·to Surface Water) o. PSO (Air Emissions from Proposed Sources) g p " " " " " E. OT_H ER (specify) C ' g 3 7 7 2 /specify) Planer Mill Cyclones " ,. ,. " " " \ E. OTHER (specify) l ach to this application a topographic map of the area extending to at least one mile beyond property bounderies: The map must show. outline-of the facility,.the location of each of its existing and proposed intake and discharge structures, each of its hazardous waste atment, storage, or disposal facilities, and each well where it injects fluids underground. Include all springs, rivers and other surface · water bodies in the map area. See instructions for precise requirements. NATURE OF BUSINESS (provide a brief description "This establishment is primarily engaged in sawing and planing rough lumber land/ or timber from logs." I I . CERTIFICATION (see instructions) nify under penalty of law that I have personally examined and am familiar with the information submitted in this application and all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information contained in the lication, I believe that the information is true, accurate and complete. I am aware that there are significant penalties f0r submitting information, including the possibility of fine and imprisonment. AME .!Ir OFFICIAL TITLE (rype or print) 8. SIGNATURE C. DATE SICNEO • Hersereau -Senior Vice President N av 1 2 1sso MENTS FOR OFFICIAL USE ONLY REVERSE -.FOf'M -3 ·oEPA CAA OATE RE.C.EIVEC r. mo. <l da U.S. ENVIR--,..,..,.MENTAL P~OTECTION AGENCY HAZARDOU' ;\ASTE PERMIT APPLICATION c. ... -.... OJidarsd P'!rmiu Program (Thia information LI required under Section 3005 of RCRA.) COMMENTS ace an "X" in the appropriate box· in A or 8 below (mark one box only) to indicate whether this is the fim acplication you are submitting for your facility c ised application. If this is your first application and you.already know your facility's EPA 1.0. Number, or if this is a revised application, enter your facility· EPA 1.0. Number in Item I above. · Fl RST APPLJCA TION (pl.o,,ce en "X" below.and pro1.1IIU the appropriate dau) ~ I. l!XISTING FACILITY (Su ln,tructio"-6 for d.eflnitton of "e.xLltinr" facility, 71 CompUlte it•m below.) • _ . l"OR l:XJSTTNG FACILITIES. l'AOVIDE THE CATE (yr., mo •• & d.o-:,) OP'ERATION Bl!:GAN OR THlt CATE. CONSTRUCTION COMMENCEC (UH the b0%•• to th• l•ft) N (place a.n "X" below and compl,tt.e item I aboue) □ 1. P'ACJLITY HAS INTERIM STATUS " . PROCESSES -CODES AND DESIGN CAPACITIES ' n2.NKW Jlll'ACI.LJTY (Complsts It.em /Hlow.) ~ ,-OR Nl!:W FACJLITJ ----------• Pl"IOVICIIE THI!: DAT (yr.,.mo., & day) ope:· TION 81!:GAN OR JS EXP't!:CTll:D TO Bl!:G· □·2. JFACli.iTY HAS A RCRA PttRMIT ., PROCESS COCE -Entar the code from the lirt of process codes below that be-st describes eech procesa to be used at the facility. Ten lines are provided fc entering codes. If more lines are need&d, enter the code(:) in the space pro-.ided. If a process wilJ be used that is not ineiuded in the lilt at codes below,ith£ describe the process (incl'!ding Its daigncapacity) in the space provided on.the form (Item lll•C). · · ~· · PROCESS OESJGN CAPACITY -F~r B8ch code &nt;red in coiumn·A enter the capacity of the proceu. ,. ,_ . .-,. ·:{:T:~~~}f~·?.:):'/.\·t;,~ ,. AMOUNT -Enter the amoont. · . ' " • , -.. · . _ . :,•::. " ·•· ._~:..;, -, .. ·.·.~ .. ~::-··, UNIT OF MEASURE -For tech amount entered in column 8(1.), enter the code from the llrt ot unit measure code:s below that describes the unit o1 ' measure wed. Oniy the units of measure that are listed below should be used. , .. ~.~, .. :ii/., .. :\:;;,·;••.- , . PRO' APPROPRIATE UNITS OF APPROPRIATE UNITS OF·· CESS . MEASURE FOR PROCESS· MEASURE FOR PROCESS .: PROCESS CODE· DESIGN CAPACID' ·. :,.. DESIGN CAPACITY· CONTAINER (b"'o.rnl,. dTum,. .ii}> sot .. ~'GALLONS OR LITERS. -:,.:· :,·-.-·.-•1 ··•":·!: TANK -; SO%."· GALLONS OR LJTE.RS -' .GALLONS Pf:R. DAY OR LITERS PER CAY .. WASTE" PJL.!!::,:_~ .~_:;,:·~:;::.: SOJ:· -CUBIC YARDS OR · .. '. .so.a·;:'.:~UABLILCO~ESTOEARSUT"RS, .:._ .. i\>\ S~f!P'AC!!: IMPCIUNO~.ENT. T02: GALLONS PER OAv·oR1 LITERS PER CAY SURP'AC~ IM_P.?UNDMENT :_-:·: -.. ,. n .., :-• • .. SURFACE IMPOUNDMENT··~. UNIT OF MEASURE .·:o71'"·-GALLoNs oR .. L1TERs ···· oao . .: ACRE-FE!!:T (the uotum.s that ~·: ... -:.would couer on.e acre to a ·, , 1 depth of ona foot) OR ., 7 HECTARE-METER ca1:-ACRES OR H!:CTARl!:S D82 GALLONS PER DAY OR LITER'S PER DAY 083., GALLONS OR LITERS· UNIT OF MEASURE · cooE· :~-.'.)'OJ·., TONS PER HOUR OR METRIC TONS PER HOUR: ·.·oTHER ({Jae for phy,lcal,· ch•mictuy tlwrrnaJ Or btolo1ical treatment proct1ue• not occurrlni iri ta.n}u.. · AJT(oce impoundm•ntl or inci~,.. ato,... De,c::rib.e tha proce.u• in . the ~po,ctJ prouiiud: It~m ll1•C.)·. · TO, ... GALLONS PltR HOUR OR ~ITERS PER HOUR GALLONS P'l!:R CAY OR · ''UTERS PER DAY · ; ·, ·:•.:.::~:::·.·.:·~\ /·})}\··:::~:-: . UNIT OF MEASURE GALLONS. ~ • .• .•; ·, .. Q. -~-LJ'TER5 PER DAY-.... • .• , , v:. ACRl!E•fl'l!:ET •• ;. . • • ., ••• LITERS • , • • • • : ;. ~ L TONS PER HOUR·. • ; ;· _. o· .·~ Hl!:CTARl!:-Ml!:TER. ..~\ .. _.~ ... ,,,.. . .. · .. , .~ ..... CUBIC YARDS. -. •.· .··' •. -.·,•.•.··.·_.;·: •• '.,~.·•.;." ·Me:TRIC TONS PER· HOUR~· _.";•:· .: /~ W ·. ACRES •. • • CUBIC METERS -C.ALLONS PER HOUR , • • • ,· .• , .·• .. ,.e:: " HIECT ARES ••. ~ •• : GALLONS PER CAY ; •. ~.: •. C:-.'·. ·_:.:;._·;.-.• : •. u, ·::·'..!: Ll~RS Ptl"R HOUR. ; ··• •; • : ·~. ~. ;;:.,"; ~·tt-· ••-·:.: · .:~ ·. ·-" . •·· ...... ·• 8 ........... Q MPLE FOR COMPLETING ITEM Ill (shown in line numben X-1 and X-·2 below): .A facility has two storage tank3, one tank can hold 200 gaUont and th ther can hold 400 9Bllon1. The facility also ha, an incinerator that can burn up to 20 gallons per hour~ · DUP B. PROC.ESS.DESIGN CAPACITY .,f. AMOUNT · (,pecif":/) 600 20 3520 " 2. UNIT OF MeA SURE (ent11r code) G E G FOR OFFICIAL USE .ONLY. a: A. PRO·+---B_._P_R_o_c_E_ss __ o_E_s_,_G_N_c_A_P_A_c_,~T_Y __ _ ~ CE:SS LI.I CODE z ~ (from lilt Jz abo1.1ef FOFi OFF'JC: 5 6 7 8 9 10 " u .. 11 a PAGE 1 OF S ·.1. AMOUNT " %. UNIT 01" MltA· SURE (~nte~ code) .. .. .. " USE ONL' CONTINUE ON REYE ROCESSES /conrinued) ·, --11¥11/i!1tffi.~ CE FOR AOOITIONAL PROCESS CC. ."J OR FOR OESCRIBING OTHER PROCESSES (c~_ .. "T04"). FOR EACH PROCESS ENTERED HERE !-UOE DESIGN CAPACITY. I I I I I ESCRIPTJON OF HAZARDOUS WASTES A.. A H O NUMB -nter the tour-ai91t numoer rom R,. Soop.art D ror eacn listed hazaraou, waste you w1 handle. If you handle hazardous YY&stel which are not listed in 40 CFR. Subpart 0, enter the four-dlgjt number($) from 40 .. _CF_R._Subpart C that describet the_cherticteri►•, ;: ·_ r -~nd~or,_th~ ~xi_c_.~n~-i~~ o~ .t~ ~-~-~~-;~~--·:. ~). ~.:.;::' :'-,"/\ -~·r~.:~•.;):·:=\),?.;_::;~;(i~t-{i/~1(.///\;);:'.;~\~\;{{)-t(t-\: \(/•.:\-~(?/!>.~:~ ·.\;; :-\)f }: B. (IT1MA TEO ANNUAL QUANTITY -For each llstad warta entered In· column A estimate-the quantity af that wasts that 'Nill be handled on an llllnual , · basis~ For each characteristic or toxic contaminant entered in column A fflimata the totm an~ quantity; of au the non-Hsted warce(i). that will be handled. . · .. ~i~ ~. ~hat '~~~r.i~i-~ ~-~. ~~~i~-~ ·.·. -~·.· )~~J\ ~):\i_;.}/f/i{: .'\-/ :~\-?(f.;.:f\.:.:°J.{,;-;;::~.:~t~<~:~i :\>}·.)•;:: .. .-i~··;_~.· :(\:;_/?;~·: \?/:t~ )(/.·./)};~it): C.. ~ OF MEASURE:_ For eech q"t,antity ·emared in coJumii. B enur the unft·of-memurv code. Untts:·af. me81Ura·which.mun bet used and tfit,.approprfatv, , •. -·. ·· ·~~~i'.;:.~'i'!~i;·;~·;,;~~0(7:6i,'.).df :l[c~~~~iiTI!,~!;;ii ;;;; .. •;~ 1,::r:::Ji~i i~I&! ·1t faeiJity recon:k use any other unit ot·measurs. for-quantity, th&-units of.ma.sun, muei·be eon~-in10-one of the rec:iuired uniu of meel!JnJ_taking Into D.,;;:~:~:::· denuty ~'. ;0:.~~;~;;;p-~i:i::7i,:,'{:f::: :.~5~-0;0~~'.'.~s~:::~?:rf!:2<~;,:-HJ:i{.:, •'•·••· i,'., '.' '. ,':;·~~::':};\:;~·::~::' For lilted hazardous wats: For ·each lirtad hazardoui waste.entered in column A sektc't the code(s}-from· th& list of procesa codes contained In ltsm 111.· .. : . to indicate how the waste will be stored, treated, and/ex disposed of at the facility. · · ·. · --~ ..,.: ··:: :::~t_:-.: ·:-: '<:::-· · ,: -.:·:: . -·. · ,.-, : ·.· .,: :.: . • •:.. ··:~· -·:<-'•<'::·-': . ·a For non-fisted hazardous wanes: For each characteristic or toxic contaminant entered in column A, select the code/1) from the list o1 process-code,. .-.:: contained in !te_m 111 ~ indic8te _all the procesaes ~~· !"i.11 ~-~-~--~o~~ -~r_a_~/°!". ~-~~-~t_. ali_:th~---.~~list~--~~~u• -~ that_ Po~~---.· _. that charectenstic or toxic contaminant. · · .. -.·.-· .. -... " , -..... •, ·-. · ·. . ~ ·. · ·· ....... · . ··-· •, - . . · . · .. . · ... -. Note: Four space, ant provided for entering_proeesl codes •. If more are.needed:··11) enter the first.three as described above; 12r Enter_"OOO-;in the·: · . .-,. e.xtreme right box of Item IV-0(1); and (31 Enter in the space provided on page 4 .. the line number an_d the-additional code(s).: · :,::'· _ ·w·-::~~ :-:-: ~, . _, ~ •· .R P~OCESS OESCA;PTJ~N: i1 .~.;~·not i;..~~o~ ~~ ,;;~ ,.;;J~F.i.d~i~~~~-i~~ ~+~;~ 0~ ;™.'fo~~"'E•·:c;rt.?::; NOTE: HAZARDOUS WASTES DESCRIBED BY MORE THAN cii.iii EPA HAZARDOUS WASTE, NUMeiiii":.,c ~rd;;.;~ ;.,;,~i u,..; ,,;,h "".deocribod by more than one EPA Hazardous Wasta Number $hall be described on the form es follows:. ..:... .. _ ... ,_.· . .-. ->.-;-..:._-_. s.,: :,:··. · ... ·: •• ,-..• · . _-·.•. _,-._. .• , ··"· ..... -.. ·~, ••.•.. _. • . o Select one of the EPA HazardQus Waste Numbers and enter-it in cdumn A. On the S21me li·ne eomp(ete C01urrm1 B,C. and D by estimating the totm annual . ·;· quantity of the waste and describing all the processes to be used to treat, store, and/or dis;pose ot the waste. . ·. . , : . ·. · -,_·-. · ' .. ·- . • In column A of the next line enter the othet' EPA Hezardou.s Wute Number that can be used to describe the waste. In column 0{2) on that line enter .. lncludedwithabove"andmaksnootherentriesonthatline. . . . .. . ·· J • " ..... ,.-., .. , •••• Repeat step 2 for each other EPA Hazardous Waite Number that an be-used to dacribe the hazardous west&. -~ ·_ . . ,_. • :. '· ·-.-;-~· __ -:_·:· ." ,--_ .. -· ·. _. _.,,.-~: · . E~ Lf FOR COMPL~~G iT~M ;~· /dr~-/~ i1n~·nu~ben ;_;~ x.i-x.a, an;~:, beJ;;,/~·i· ~~ci·;ity ~II -tr~\~ ~is:.~~~ esti~,~ed ~~~nm· ~ r of ehnJf'ffll shnings from leat~ tanning and fini.shiog operation. In addition, the facility will treat and dispo-se of three non-listed wSstes. Two waste, are corrosive only and there will be an ntimated 200 pound, per year of each WBSte. The other w:asta is corrosive and ignitable and there will be an estirnat&d 1 nds per year of that waste. Treatment will be in an incirterator and disposal will be in a landfill. A.EPA C.UNIT C. PROCESSES "' ~AZARC. B. EST1MAT'ED ANNUAL 0~ ME.A z· ASTE NO QUANTITY OF WASTE SURI!: f. PROCESS CODltS 2. PAOCE"SS OESCRl~ION ~ (enter code) (anter (~ntar) ·· · (If a cod•'-not entervd In D( 1 )) co") I I I I I I I I K o 5 4 900 p T 0 3D80 I l ' 7 ,7 ' ·' I ~ D o o 2 400 p T o 3 D8 o ' I I I ' ' ' x_ D o o 1 100 p TO 3 D8 o _xlD ' I I I I r ' I o o 2 included with above ,?A Fann 3510-3 16-801 f'("HUTIJIJI IC f"'IJIJ C/\r.:C A.EPA HAZARD. Zo WASTENO J z (enter code} B. ESTlMATED ANNl.JAL QUANTlTY OF WASTE .. .. .. K 0 0 1 16,300 D 0 0 0 20.000 D 0 0 7 D 0 0 8 5 F 0 0 1 375 F O O 3 F 0 0 5 10 I ~ ~.tZ-1-------C--------_;._;C::·:..Pc.:..:R::O:;C::..:E::S::S::E::S:._ ____________ _ SURE (tinter coda} .,. I p a p p ·. l. PROCz=~9 COO ES , (•nt«rJ 1 I , 1 1 I l S O 1 ' ' ' ' ' ' ' s O 1 ' ' ' . ' . ' ' ' ' ' ' ' ' ' ' S 0 1 ' ' ' ' ' ' ' ' ' ' ' ' ' I ' ' ' I I ' ' ' ' ' ' . I ' ' ' ' ' ' 2. PROCESS OE.SCRtPT10N · (If Q code ~ /'1.Ct t1ntt1rcd In D( 1)) · Included with above Included with above Included with above Included with above ,_2_·i· -t-+-+---+------------+'_:{.,;'.f-+>~··-c··· f-.-:7:r-t-7,-.-:+-,--:.-+-,,-.-:+-------------------- 13 14 ·., ' ' . . ' I I ' ' . ' ' ' ' ,-:-· +-++-+-l------------+-:.-'-.l--t•'-..• _JO•l-~,T,-l-~,T,--l-,r-~+-~-~,+------------------- 1 - ' ' ' I ' ' ' ' ' ' ' ' ' ' ' I I I I ' ' ' ' ' ' ' 0 ' ' ' ' ' ' ' I I I I ' ' ' ' 2 ' I ' ' ' 23 ' ' ' I I I I I 4 I I I I I ' ' 6 ' ' ' ' ' ' ' t't U?7•nn•ttt4 u CONTINUE ON REVE: PAGE3· __ OFS (enter "A", "B ", "C", etc. behind the "3" ta identify photocopied page•) IV DESCRIPTION OF HAZARDOUS v· .. -TES {cor.rinued} j2"~ tsE TnlS SPACE TO LIST AOOIT AL PflOCESS COO ES FROM ITEM 0( I) C. I I I I I AC!LITY DRAWING \'t~fi&fflitt!Pt~ AGEJ. ' -. All existing facilities must include in the ~pace provided on page 5 a scale drawing of the f_aci!ity (see insrructions for more derail). VIHOTOG RAPHS )WS!RE¥ii&ii-i@ ""'9@tfii&HiH&¥&¥ii¥ A xi sting facilities must include photographs {aerial or ground-Jew,/} that clearly delineate all existing muc:1ures; existing storage, treatment and disposal areas; and sites of future storage, treatment or disposal areas (see instructions for more derail}. FACILITY GEOGRAPHIC LOCATION FACILITY OWNER If the facility owner is also the facility operator as listed in Section VI 11 on Form T, "Generai Information", place an "X"' in the box to the left and skip to Section IX below. · -· · · -· · ... If the facility owner is not the faciiiry operator as listed in Section VIII .on FOrm 1·, complete the following iU!ms: t. NAMI!: OP FAC1LJTY'5 L.ECAL. OWNER 2. PHONE NO. (area cod~ & no.) . .. H 1' • It " .. 3. STREET OR P.O. aox. 4.. CITY OR TOWN 5. ST. 6. ZIP COOE GI I I .u. IX. OWNER CERTIFICATION 1 IJy under penalty of law that I have personally examined and am familiar wirh the information s.ubmirred in rhis and all attached do enrs, and that based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the sue itted information is true, ac::urate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment_ • A. ,ME /print or t:;peJ B. SIGNATURE C. DATE SIGNE □ S. ~ersereau NOV 121980 ERA TOR CERTIFICATION ify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached dccuments, and rhat based on my inquiry of those individuals immediately responsible for obtaining the information, I believe rhat the su,,., itted information is true, accurate, and complete. I am aware that there are signific:;nt penalties for submitting false information, · ' ing the possibility of fine and imprisonment. ,I\. NAME (;}l'int or type; I S. Mersereau ;p..., rm 3510-J (6-30) B. SIGNATURE PAGE40F5 C. DATE SIGNE □ NOV 1 2 1980 CONTINUE ON PAG=: Con:inu'ed frOm page 4. 'i. FA'CILITY'DRAWING (see page 4) ~-Fo,m App,o,ed 0MB No. 158-S80004 'PA Fo,m 3510-3 (6-801 ~£1.Zr.=JRDO.U.S _ -//.IR5 T.(:;.-_ STORl?c;;t: ~ (ec,',<zo') v __ 2,C..,9/1..,I_E,f:' __ _ I I I r ________ _!G,.-i;:C:i,;O!J,3,,.. ·PACU'lC CORPORA T!O,f 3 so;-;•':;;:,;-;1/c;--------______ , ~ P. 0. tlbX !SOB "'9i!:' I'/( '-1\, Al.!C\JSTA, GEOllGlA 309© PAGESOFS I I I I I I ,, I I I I I I I DIVISION OF HEALTH SERVICES P.O. Box 2091. Raleigh, N.C. 27602-2091 Mr. Gerald W. Tice Georgia-Pacific Corporation P.O. Box 1808 Augusta, Georgia 30903 Dear Mr. Tice: REF. 10 Date: August 11, 1982 Re: Facility ID No. {.//~ . oc:··;nald H. Levine, M.D., M.P.H. STA TE HEAL TH DIRECTOR NCD000813592 Based on infonnation suppl led by you we have processed and accepted at the State level your·request for the facility identified with the above ID number to re- ceive the indicated change in classificat i.on under RCRA: Add As Delete As ------ D 0 genera tor D □ transporter □ □ treater □ ~ storer □ D disposer [81' □ small generator We arc aclvisinp., EPA o[ the chcmg"c in your status. any f11rther change in your operations whic:h would Your EPA ID NO. is D is not~ being cancelled. Please notify us if there is ;1gnin affect your status. 01-1S cc: John Herrmann· EPA Region IV Emil llreckling Fred Wood DIIS form 3048 3/82 Soli.<l & lbz. Waste Mg t. Branch Cordially, (O~~ 0. W. St n.c kl::rnd, i?e::'d Solid & Hazardous Waste Management Branch Envi ronmen cal_ Heal th Section \ I STATE,OF NOR:TH CAROLINA Jorn;:·, fl Hur'!, lt/·ocr~-..RitAENT Of HUMAN RcSOU~Ct:S ~-oruh f ,'.\oOION, .',\D, :.,PH 1 GOVFRNOi-1 ~EUEfAqy ·-·-····-------·--··--------·--------------·----------··---------------·-----·---·---·-----·-·-··-.. pp-• p...,._ REF. 11 · NORTH CAROLINA HAZARDOUS WASTE MANAGEMENT RULES and SOLID WASTE MANAGEMENT LAW DEHNR DIVISION OF SOLID WASTE MANAGEMENT HAZARDOUS WASTE SECTION P. 0. BOX 27687 RALEIGH, NC 27611-7687 · (919) 733-2178 January 1, 1995 State of North Carolina Department of Environment, Health, and Natural Resource■ Jam.ea B. Hunt, Jr., Governor Jonathan B. Howe■, Secre~ Property of _____________ _ Address Telephone This Book is manufactured of a High Grade 50% Rag Paper having a Water Resisting Surface, and is sewed with Nylon Waterproof Thread. 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" ·····---·------1-----1------ ------· ----------1-----1-----11---- ----~--------1-----1-----1----- _____ , _____ , ______ ------ . ·----------------1------1-----1----- ----------------1------1 ~%·:.:--.. i~~it ·,.. £::..,·_ ~~-'. !:.';B'~~-"' '.....:..:~'ll.. -__ ._;_., -~. ,:•-~~':; ., ~-... •-)_ ~.: .a: I--------- REF. 13 • - I POTENTIAL HAZARDOUS WASTE SITE L IDENTIFlCATION oEPA PRELIMINARY ASSESSMENT 01 STA.TE,0.Z SITE~ NC D000813592 PART 1 • Sl'TE INFORMATION AND ASSESSMENT I IL SITE NAME AND LOCATION Qt $tT'E~a...--------..., 02 STREET. JIOJTE NO-. 0A SPl0FlC 1,.DCA~ ICEHTlFEII Georcria-Pacific Com. -Hard\=:xi Sav.mi.11 Pl -Dr..: ...... o,cm OASTATE 001JPC00E OOCOIMTY 07~, QICONO I C00E asr Plyrrouth NC 27962 Washington 094 01 oa COORCtNA TES LAnTUCE I LONGll\JDE -· I 35..... .52-2.li.... ..O'.ZE-44-:ZS.... 10 Ol=tECTIONS TC SITE~._ __ ,..__ · Fran East Main street in Plym:,..ith, turn north onto Pl~ Drive and go amut 1500 feet to the site. I -. -- DL RESPONSIBLE PARTIES 010WNER,. ....... ·-· -· . -028T111EET--. ...... ,__. ' I Georgia-Pacific Coro. ·• .. P.O. Bax 105603 .. -. o.scm . -. -··· . ----CM STATE CO 1J1' CODE 00TEL.EPN0NE......,, Atlanta ---..... GA 30348 404 l 521-4000 I 07 OP£RATOR ,. __ .,,.,.... _ _, .. ·-----· Dl&TREET-.--.. __. --·-· . .. - 011cm --... : 1OSTATE 11 ZIPC00E , 2 1'E.D'H0NE .....asER I .. . _ . ._ . ( ) - 13 TYPE OF OWNERSHIP ,o...__, II( A.. PRIii A TE □ B. FEDERAL.: □ C.STATE □D.CCUNTY □ E. i.aJNICIPAL --I □ F.Oll!ER: □a.UNKNOWN ' ' 14 OWNERIOPEJIIATOfl NQlPCATION ON A..1.0,.,. •-~ . ---- ll!!A..ACRA300I DA~RECSi/EO: J J ,J2 BO C L LWC0NT'R0U.ED WASTESITE,clJICI.A tNc DATE RECEIVED: . . □ C.NOtE IOfflol 0.Y ftM W0HTN Q&'f ftM I N. CHARAcnRIZATION OF POTEHT\AL HAZARD-'-·--.-·- 010N~NSPECTJON ----.-,. IIYO-•-__,, · ... ; . . □A.EPA. □ B. EPA CONTRACTOR □ C.STATE □ D. OTHBI~ --. -- □YES DATE ----. □ I!:. LDCALIEAl.nl OFRC1A1. □F.O'THBI: .. )QNO . ...,. DD'.,.... -·· -- I ·---·~·--CCINTIIACTtllfNME(S): -· . . . .. 02 SITE STATUS~--GlffAMO,CPBIATDll -. ---·--·-:..-.. □ A. ACl1IIE □ B. IW:'TIIIE .. ji·c. -. ·_. . ---.. :· .. .. Pre iqso I □UNKNOWN ,. --· -·--· .. - I _,.... ........... 04 0ESQIIPT'ICIN o, IUDTANCE.a PClllal.Y l'fl!SENT. JCNOWN. CIIIA&J.212D . '1ru.s facility was-purchasea ftau Atias -p1 ywcod in 1950. 'lbe ex:isti.o, buildin;s \.ere .. danolished·and new str=tures:l::utlt:-..0.---j>.fter a fire in 1983, the plant was pe=anenily ·- I closed. Reportedly; Georgia-Pac~. -1~ owns the site. .. 06 OEacM'TCIN o,; ~ NA.ZM1D TO BJMC I IBff NGfalll'CIP\LAlDt Since the facility has been :i.I, opeLdL...00 for at least 35 years, and since pre-1950 pi:cxe.: I and waste hamliD;. practices are-uix::Iear; this site ~s a tine-available on-site·-- inspection. I ..•.•. ·---· :-•·· ·--· ·/--.. -:-: • -· .. ., .. . ..... -- ' . -· .. .·• Y. PRK>RJTY ASSESSIIEHt -. I 01 ~PCftNSI ECII.IN,.:a.--•---•--•------;,._•~------~••O.-...-'WC:.....W---- □A..HDH CLMBIUol C.LC1W CD.NONE . .. ·-,...._...,........,. . ------.. _____ ......... ,.. ___________ ...., I VL INFORMATION AVAD AIII EFROII . . ··-- 01 CONTACT .... ,. .,. TEI.EPIOE- Tern Stevens, Enviro. Enaineer Georcria-Pacific Co,..,.,. 14041 521-5080 °' PERSON R£SP0NS1a1..E FOR ,sac:nrrrr .. _.. DI c:Jfll»NV,TIQN 07 T£L.EPtt0Nt.....ulEII ooi,,.Tl I Grover Nicholson NC DHR/D!E SHW »:;int. Br. 819 1733-2178 ]2 ~lfi ,85 ..:.tTN °'" ftM EPA fOP,M 2070-'2 (7 .. 11 l -·---·.J - \ .-. -:, \ ·'--: -:. , . ; ~; . --:. __ -::.:..(·--v-------------/.". --/ . ' "' _____, ) ,t:Y-y _,...,,, _.r ; ' -' ' I I , ···<'' I I •• I J ,, .. 1:..: r.~:;;::.--,,, / L.,,,..,,, . ....__,-, I .·, -·-~--.-, ,, . _,. ,,.- (_,f, ~-C::::~=~ . ----.:.-J?~r; } I-~'.;,~~~:_ ·-· · . _. .---~~~:a; "'21 ::·.-·~.i.~ -t- ~ __., ...---,, ~:...-. ,._{ ~ I -~ :, . •• -4 ,_, . ,., .~--) ,-,I,,_; . / . "".,-- \~/ . ... --~ '' .. I ,,,--.....,_ I 1 ,q , . ' t) \ ~~ • I : .,,,.: . •1 . '"'x~ I I ,---\ fi~ . .. _/ .. :· ~o\ •• ·-J:~:i1 ~-. I : ~"-"' "I, ••O 197' ••G•<T<C •0"" . 1--------........ " 0, -~---~~ :-:~ - - NORTH CAROLINA 7.5 MINUTE SERIES (TOPOGRAPHIC) ---::::::::,;.___: ' SCALE 1:2400J CONTOUR INTERVAL 5 FEET NATIONAL GEODETIC VERTIC,t,L DATUM OF 1929 StlOAE.LINE SI-IOWN REPA(S[NIS IHt APPRu•1MAI( ll"'[ uF ,,.lAN .. ,i; ... WAl[A l1-1( M[AN JU.NGf. Cf TIO[ IS l(SS TH"N ', fC'QI ~-- ,_; --J· NUS REF. 14 CORPORATION _ 7 LAKESIDE PARKWAY SUITE 614 TUCKER. GEORGIA 30084 ,-938-7710 I ID I d 1n I~ I 1' Ii II II II I --1 11 11 11 ,. '-ii !JI August 20, 1990 Mr. A. R. Hanke Date: Q I C-586-B-0-165 Waste Programs Branch Site Disposition: .:_: . ..:~.·-1· f· b:Ll~ ~2 Waste Management Division Environmental Protection Agency 345 Courtland Street, N. E. Atlanta, Georgia 30365 EPA Project Manager:)) i.-~r·, \ c+-' r-... \, ~r-:. r (..: .. J Subject: -· · Screening Site Inspection, Phase I Georgia Pacific Corporation Hardwood Sawmill , Plymouth, Washington County, North Carolina EPA ID No. NCD000813592 TDD No. F4-8909-89 Dear Mr. Hanke: '--' ~ FIT 4 conducted a Phase I Screening Site Inspection at the Georgia Pacific Corporation Hardwood Sawmill located in Plymouth, Washington County, North Carolina. This assessment included a review of EPA and state file material, completion of a target survey, and an offsite reconnaissance of the' facility and surrounding area. The Georgia Pacific Sawmill is located on Plywood Drive in Plymouth, North Carolina. Geographically the facility is located at 35°52'35" N latitude and 76°45'30" W longitude (Ref. 1). The 25-acre tract of land on which the facility is located was purchased from Atlas Plywood in 1950, whereupon the pre-1950 structures were demolished, and the planer-sawmill-office building complex was constructed. After a fire in 1983, the plant was permanently closed (Refs. 2, 3). Currently, the Outer Banks Contractors, Inc., Plant Number 4, makes asphalt at the Plywood Drive address and is owned by Decatur Partnerships of Naggshead, North Carolina (Ref. 4). Operations at the Georgia Pacific facility included the production of treated and nontreated hardwood lumber (Refs. 3, 5). Process wastes associated with the plant consisted primarily of spent oil (D000-ignitable/D007-chromium, D0OS-lead), spent halogenated degreasing agents (FOO 1 ), spent nonhalogenated solvents (F003, FOOS), bottom sediment sludge from the treatment of wastewaters from the wood preserving processes, and an insecticide formulation. The preservative used, Noxtane (trade name), was manufactured by the Koppers Company of St. Louis, Missouri and contained pentachloropheneate, sodium metaborate, and other chlorophenols. The insecticide formulation contained lindane (Refs_. 3, 5, 6, 7). During the process of wood preserving, lumber was passed through a dip vat on a conveyor system. After removal from the preservative or insecticide formulation, the wet wood was allowed to drip dry onto the ground, thus contaminating the soil (Ref. 3). Annual waste production at the facility included 20,000 pounds of D000, D007, D00S waste, 16,300 pounds of K00l (bottom sediment sludge from the treatment of wastewaters from wood preserving processes that use pentachlorophenal) with lindane, and 375 pounds of FOOi, F003, FOOS waste (Ref. 5). A RCRA Part A application indicated that the wastes were stored in drums (Ref. 5). I B I D I '0 I ID I~ i~ I UI 11 I I I I i I I I •• •1 • , 1, 1, 1.1 ••• I Mr. A.R. Hanke Environmental Protection Agency TDD No. F4-8909-89 August 20, 1990 · page two During a RCRA Inspection conducted in October 1981, representatives from the North Carolina Department of Human Resources (~JCDHR) discovered that the wastes were being burned in the facility boilers and/or sent to the county landfill (Ref. 3). It was also noted during the inspection that the wood treatment process involved spilling waste directly on the ground (Ref. 3). A tank used in the wood treatment process was also found to be leaking (Refs. 7, 8). Remedial action plans were initiated by NCDHR in November 1981, but no removal has yet taken place (Refs. 9, 10, 11 ). The facility submitted a RCRA Part A application for a hazardous waste permit on November 12, 1980 (Ref. 5). In August 1982. the facility's status was changed from a treatmenUstorage/disposal (TSD) and generator facility to a small-quantity generator (Ref. 12). According to NCDHR representatives and file material, the Georgia Pacific facility is currently listed as a conditionally exempt, small-quantity generator due to its inactive status (Refs. 11, 13). The Georgia Pacific Hardwood Sawmill facility is located in the Atlantic Coastal Plain hydrogeologic regime. This regime cons1Sts of complexly interbedded sand, silt, and clay overlying unconsolidated sand, silt, and clay. The slope of the interlayered beds toward the ocean controls groundwater flow (Ref. 14). Washington County has a moist, temperate climate with a net annual rainfall of 7 inches and a 1-year, 24-hour rainfall of 3.5 inches (Refs. 15, 16). East of Plymouth, in the town of Roper, the formations found in cross section are 15 feet of surficial deposits, 200 feet of sand and marl of the Yorktown Formation, and the limestones of the Castle · Hayne Formation. The section is shown to thin as one goes from east to west; however, one can extrapolate that although the Yorktown Formation will be thinner, it will exist underneath Plymouth (Ref. 17, p. 56). The surficial deposits are rarely used as sources for potable water. Domestic wells sometimes use the Yorktown Formation for potable water sources (Ref. 18). The aquifer normally used in the northwestern part of Washington County is the Castle Hayne aquifer (Ref. 17, p. 53). This aquifer consists of limestone and sand and is generally confined. Regionally, it is found 70 to 200 feet below land surface (bis) (Ref. 19). Well depths in the Plymouth area range from 110 to 214 feet deep. More recently, in western Plymouth, the Castle Hayne aquifer is found 150 feet bis. Through artesian effect, the water levels were either flowing above ground or less than 10 feet bis (Ref. 17, pp. 55, 76, 77). Because of much withdrawal from the aquifer, the water level is now about 28 feet bis (Ref. 20) The layer of marl and sand found in Plymouth represents the layer of lowest hydraulic conductivity between the aquifer and the surface. Marl and sand of this type have been shown to have hydraulic conductivities thatrange from 1 x 10-5 and 1 x 10-7 cm/sec (Ref. 21) . Residents within the study area obtain their water from one of three sources: the city of Plymouth Water Works, the Washington County system which obtains water from the city of Plymouth Water Works, and private well use. The city of Plymouth Water Works uses of four wells having an average depth of approximately 175 feet and two water tanks having capacities of 250,000 and 500,000 gallons (Refs. 1, 22). The four wells are located between 1.3 to 2.0 miles from the facility and serve 5,000 people. The county system serves 3,900 people, including residents in a limited area adjacent to the city of Plymouth (Refs. 1, 23). Private well use within the 4-mile radius is limited to 108 residences located near the periphery of the 2-to 3-mile radius and 337 residences located within the 3-to 4-mile radius, making the total private well use within the 4-mile radius 445 residences (Ref. 1). Private wells within the study area are generally 200 ± feet deep (Ref. 22). The closest private well is located on Route 1 approximately 2.7 miles from the facility (Ref. 1) . NUS CORPORATION Mr. A.R. Hanke Environmental Protection Agency TDD No. F4-8909-89 August 20, 1990 -page three Judging from the topographic relief, the Georgia Pacific facility is most probably located in a flood plain (Ref. 1 ). Surface water runoff from the facility would flow 530 feet overland to the Roanoke River, then continue 6 miles to Albemarle Sound (Ref. 1). No surface water intakes are located along the IS-mile extended migration pathway (Ref. 24) Recreational use of local waters includes swimming, fishing, and boating. Access to the facility is limited by fencing and a gate guardhouse (Ref. 21). The nearest residence is located approximately 700 feet east of the facility (Ref. I). The local high school and a Dixie Youth League baseball park are located in the residential area adjacent to the facility (Ref. 21). Approximately 2,700 individuals live within 1 mile of the facility, and the total population for the study area is 7,477 (Refs. I; 13, 25). Land northeast of the city ·of Plymouth and north of the Roanoke River is primarily uninhabited freshwater wetland (Ref. I). The bald eagle (Haliaeetus leucocephalus) is a federally and state-designated endangered species found in Washington County. Additionally: the Waccamaw killifish (Fundulus waccamenis) and the golden eagle (Aguila chrysaetos) are state-designated endangered and threatened species, respectively, that are found in this county (Ref. 26). Due to the low probability that drinking water will be impacted by wastes associated with the prior operations, it is the opinion of FIT 4 that no further remedial action be planned for the Georgia Pacific Corporation Hardwood Sawmill facility. If there are any questions concerning the information contained within this report, please contact me at NUS Corporation. Approved: LTM/gwn Enclosures cc: Robert Morris NUS CORPORATION , I .. •' '' , .... '; ' .,, I I I 1• I I I I I I I I I I I I D I I I I I I I I I r~ .,;-·..,,a~•·"'•..;~\. Mir; 1 "-~:i' 1.:" '~rnfh.··" .· i;i -~ . "" .. ~, t\ '~ I VI · . i n~ . .. : .,,,~ . -.,.• State of North Carolina Department of Environment, Health; and Natural Resources Division of Solid Waste Management P.O. Box 27687 · Raleigh, North Carolina 27611-7687 James G. Martin, Governor William W. Cobey, Jr., Secretary Ms. Kathy Amoroso Apr i 1 2 2, 19 9 2 EPA NC CERCLA Project Officer EPA Region IV Waste Division 345 Courtland Street, NE Atlanta, Georgia 30365 RE: Phase II, Screening Site Investigation Georgia-Pacific Hardwood Sawmill Plymouth, Washington County, North Carolina NCD 000 813 592 Dear Ms. Amoroso: William L. Meyer Director Enclosed herewith is the Phase II, Screening Site Investigation (SSI) Report by Greenhornc & O'Mara, Inc. for Georgia-Pacific Hardwood Sawmill (NCD 000 813 592). Based on the information gathered and presented in this report and on the results of the data validation, it is believed that the site may pose a threat to the public health and/or the environment. The following discussion of the analytical results from the Phase II, SSI sampling event for the subject site, reflects data validation. A total of nine (9) environmental samples were collected to characterize the site. To characterize whether a release of contamir1ants has occurred, a limited subsurface and sur[icial investigation was conducted to obtain ground water, soil and sediment samples for laboratory analysis. The sampling locations are shown on Appendix A, Figure 2b. Tl1ese samples consisted of three (3) ground water samples, four (4) soil samples and two (2) sediment samples. -1- An Equal Opportunity Affirmative Action Employer I I I I I I I ~· I I I I I I I I I I n I D I R I I, E I I I\ Soils A background surface soil sample (GWSS0l) was collected at the site. No Purgable Organics were reported above CRDL in this sample. No Base Neutral Acid Extractables (BNAs) were reported above CRDL in this sample. No PCBs or Pesticides were reported above CRDL in this sample. See Table 1 for the inorganic results. A composite soil sample (GWSS02) was collected in the green chain area at the site. No Purgable Organics were reported above CRDL in this sample. Pentachlorophenol (690J ppb), chrysene (l00J ppb) and benzo[a]pyrene (l00J ppb) were the only BNAs reported in this sample. A qualifier of ''J'' indicates that the concentration was estimated. Alpha BHC (640XE ppb), beta BHC (77XP ppb), delta BHC (560XE ppb), gamma BHC (lindane) (1200XE ppb), 4,4'~DDT (170 ppb) and toxaphene (450XJP ppb) were the only PCBs or Pesticides reported in this sample. A qualifier of ''X'' indicates that the contaminant may or may not be present. A qualifier of "E" indicates that the contaminant value may be semi-quantitative. A rerun of this sample gave Alpha BHC (470 ppb), beta BHC (78U ppb), delta BHC (480 ppb), gamma BHC (lindane) (980 ppb), 4,4'- DDT (170C ppb) and toxaphene (l000U ppb). A qualifier of ''C'' indicates that the contaminant concentration is confirmed by GCMS. See Table 1 for the inorganic results. A composite soil sample (GWSS03) was collected in the transformer station area. No Purgable Organics were reported in this sample. No BNAs were reported in this sample. Aroclor 1254 (1.08 ppb) was the only PCB and/or Pesticide reported in this sample. See Table 1 for the inorganic results. The first value in parenthesis is for totals and the second value is for TCLP. A composite soil sample (GWSS04) was collected in the TCE area. No Purgable Organics were reported in this sample. No BNAs were reported in this sample. No PCBs and/oL Pesticides were reported in this sample. See Table 1 for the inorganic results. An observed release to soils has been documented from the data gathered relative to the soil samples. It appears that there are releases of alpha BHC, delta BHC, gamma BHC (lindane), 1,4'-DDT, Aroclor 1254, arsenic, barium, calcium, chromium, cobalt, copper, lead, magnesium, manganese and potassium. Even though the inorganics reported in the soil samples were within naturally occurring concentrations for inorganics in the Eastern United States, the presence of arsenic, chromium and copper raises concern of possible past CCA treatment even though there is no knowledge of this treatment ever occurring at the site based on available information. Sediments A background sediment sample was not collected at the site. -2- I I :I \ I I I I I I I I I I I I 0 I u I I I I I I I A sediment sample (GWSEDOl) was collected from a ditch adjacent to the lumber stack area. No Purgable Organi~s were detected in this sample. No BNAs were reported in this sample. Aroclor 1254 (0.30 ppb) was the only PCB and/or Pesticide reported in this sample. Barium (27/0.42 ppm) and lead (27/non-detect ppm) were the only inorganics reported in this· sample. All inorganics reported in this sample were within naturally occurring concentrations for inorganics in the Eastern United States. A sediment sample (GWSED02) was collected from a ditch adjacent to the TCE area. No Purgable Organics were reported in this sample. No BNAs were reported in this sample. No PCBs or Pesticides were reported in this sample. Arsenic (9.8/0.05 ppm), barium (45/0.62 ppm), cadmium (160/non-detect ppm) and l~ad (20/non-detect ppm) were the only inorganics reported in this sample. All inorganics, except for cadm-ium (0.01-0.7 ppm), reported in this sample were within naturally occurring concentrations for inorganics in the Eastern United States. Even though a background sediment sample was not collected, it is assumed that an observed release to surface waters relative to sediment samples is documented from the data gathered relative to sediments samples. Both of these ditches lead to the Roanoke River. It appears that there is a release of Aroclor 1254 and possibly arsenic, cadmium and lead to sediments. Ground Water A background ground water (GWGWOl) was collected at the site. No Purgable Organics were detected in this sample. Dietl1ylphthalate 2J ppb) was the only BNA reported in this sample. Heptachlor (0.31 ppb) and alpha chlordane (0.28 ppb) were the only PCBs and/or Pesticides reported in this sample. See Table 2 for the inorganic results. A downgradie~t ground water sample (GWGW02) was collected in the green chain area. No Purgable Organics were reported in this sample. No BNAs were reported in this sample. Alpha BHC (0.12 ppb), beta BHC (0.045J ppb), delta BHC (0.13 ppb) and gamma BHC (lindane) (0.32 ppb) were the only PCBs and/or Pesticides reported in this sample. See Table 2 for the inorganic results. A downgradient ground water sample (GWCW03) was collected in the TCE area. Chloroethane (990 ppb) and 1,2-dichloroethene (total) (19J ppb) were the only Purgable Organics reported in this sample. Naphthalene (lJ ppb), diethylphthalate (2J ppb) and pyrene (lJ ppb) were the only BNAs reported in this sample. No PCBs and/or Pesticides were reported in this sample. See Table 2 for the inorganic results. An observed release to ground water has beP.n documented from the data gathered relative to ground water samples. It appears that significant releases of alpha BHC, delta BHC, gamma BHC I I 1• I I I I I I I I I I I I I I I I D I I I I I I I (lindane), chloroethane, 1,2-dichloroethene (total), arsenic, beryllium, manganese and sodium have occurred at the site. As can be seen from Table 2, several of the inorganics are greater than the NCMCL and/or MCL. These contaminants are not known to be attributable to site activities, but the presence of arsenic in significant concentrations raises c6ncern over possible past site activities (CCA treatment). Based on the information gathered and presented in this report, it is believed that the site may pose a threat to human health and/or the environment, therefore, the North Carolina Superfund Section is recommending that the site move on to the next stage of the pre-remedial process. This investigation should focus on identifying whether contamination to surface waters has resulted from runoff from the site. Further information must be gathered on past activities at the site to better identify whether CCA treatment has ever occurred. If you have any questions, please contact me at 919-733-2801. erely, ;}½ ,,,._ C /J,-;,t._, i --- er Nicholso,, Head _on_racts Management Branch Enclosures -4- I 11 1, I SOILS TABLE 1 GEORGIA-PACIFIC NCD 000 813 592 I NATURAL RANGE GWSSOl GWSS02 GWSS03 GWSS04 I =~~~~~==:---~~~~2-------~~~~2-----~~~~2-----~~~~2------~~~~2 __ I ALUMINUM . ANTIMONY I ARSENIC I BARIUM BERYLLIUM I CADMIUM CALCIUM I CHROMIUM I COBALT COPPER I IRON LEAD I MAGNESIUM I MANGANESE MERCURY I NICKEL I POTASSIUM SELENIUM I SILVER SODIUM II THALLIUM D VANADIUM \ZINC D CYANIDE \NOTES: 0.7->10% <1-8.8 <0.1-73 10-1500 <1-7 0.01-0.7 0.01-20% 1-1000 <0.3-70 <1-700 0.01->10% <10-300 0.005-5% <2-7000 0.01-3.4 <3-700 0 . 0 0 5 - 3 . 7.% <0.1-3.9 0.01-5 0.05-5% <7-500 <5-2900 7000 5600 NA 20UR 20UR NA 3U JU 32/0.07 29 320 .220/1.0 0.26 0.34 NA lU lU U/0.08 580 79000 NA 8.1 8. 3 40/U l.3U 5.3 NA 3. 0 23 NA 6900 5600 NA 5.8 33 110/U 380 3600 NA 42 850 NA 0.29U 0.28U NA 4 . 1 9.8 NA 470 1800 NA 0.26U lU u 1. 3U 1. 3U u 250U 480U NA 0.53U 0.53U NA 13 11 NA 29 81 NA u u NA I 1 ) 2 ) 3) 4 ) 5) NA -NOT ANALYZED N -PRESENCE OF CONTAMINANT PRESUMED J -CONCENTRATION ESTIMATED U -NON-DETECT B -CONTAMINANT FOUND IN. ASSOCIATED BLANK 6) R -DATA UNUSABLE I I I I •;· NA NA 10/0.02 30/0.58 NA u NA u NA NA NA 20/U NA NA NA NA NA u u NA NA NA NA NA I I 1• TABLE 2 GEORGIA-PACIFIC NCD 000 813 592 I WATER WATER NCMCL MCL GWGWOl GWGW02 GWGW03 I INORGANICS (PPB) (PPB) (PPB) (PPB) (PPB) I ALUMINUM 300000J 690000J 20000J I ANTIMONY 10/5 42UR 42UR 42UR \ ARSENIC 50 2UJ 6UJ 43J • BARIUM 1000 5000 lOOOJ 2900J 960J BERYLLIUM 1 2J 12J lUR \ CADMIUM 5 5 4UJ 4UJ 4UR • CALCIUM 130000J 170000J 210000J CHROMIUM 50 100 340J 740J 81J I COBALT 76J lOOJ llJ I COPPER 1000 1300 llOJ 270J 31J IRON 300 310000J 340000J 71000J LEAD 50 50 270J 170J 140J \MAGNESIUM 25000J 40000J 28000J IMANGANESE 50 1300J 6000J 4300J MERCURY 1.1 2 1.7J l.5J 0.20UR tNICKEL 150 100 150J 420J 52J OPOTASSIUM 20000J 49000J 36000J SELENIUM 10 50 lUR 20UJ 2UJ !SILVER 50 SUR SUR SUR SODIUM 8000J 6500J 96000J DTHALLIUM 2/1 2UJ 2UJ 2UJ DvANADIUM 540J 920J 42J \zINC sooo 330J 940J 320J •rYANIDE 154 200 U U u • NOTES: I I I I I I 1) NA -NOT ANALYZED 2) N -PRESENCE OF CONTAMINANT PRESUMED 3) J -CONCENTRATION ESTIMATED 4) U -NON-DETECT 5) R -DATA UNUSABLE 6) B -CONTAMINANT FOUND IN THE ASSOCIATED BLANK 7) NCMCL -NORTH CAROLINA MAXIMUM CONTAMINANT LEVEL 8) MCL -FEDERAL MAXIMUM CONTAMINANT LEVEL I I I I I I I I I I I I I I I 0 I D I D I I ~ I ml I I I I I 'MEMORANDUM TO: File FROM: G.Doug Rumford r!Jf!!:) DATE: 10/31/96 REF. 16 SUBJECT: Georgia-Pacific Corp. Hardwood Sawmill Plymouth, Washington County, NC NCD 000 813 592 Telecon with Mark Wassersug of Georgia-Pacific Corp. On this day I spoke with Mark Wassersug of Georgia-Pacific Corp. in Atlanta, GA (404- 652-6871) regarding the former hardwood sawmill site in Plymouth, NC. Mr. Wassersug informed me that the facility was closed in 1983 following a devastating fire that leveled several buildings. The entire 24 .11 acre property was then deeded to Decatur Partnerships by Georgia- Pacific Corp. on January 2, 1985. Hazardous waste types and production rates were constant during the years of operation at the plant (1950-1983). However, hazardous waste disposal practices at the site are unknown. The sawmill was served by an on-site production well and septic system during the period of operation. Seventy-five workers were employed at the plant. REF. 17 United States Geological Survey Water-Supply Paper 2242 a ,r,"f;~"': .. -1'~;: s~i.t ,~r 10. ATLANTIC AND GULF COASTAL PLAIN ><,a (Complexly interbedded sand, silt, and clay) ~.: ~t\, The Atlantic and Gulf Coast~] Plain region is an l ';f,_f;• area of about 844.000 km' extending from Cape Cod. (~·-, Mass., on the north to the Rio Grande in Texas on the ,,~~(_.;_ south. This region does not include Florida and parts of (t __ ;.~--the adjacent States: although t.hose ar.eas are~ part o.fthe (,,' · Atlantic and Gulf Coastal Plain phys10graph1c province, ¥;t.t~ they together form a separate gro~nd-water region. (See 11:-t~ region I I, "Southeast Coastal Plain.") il .,,.... The Atlantic and Gulf Coastal Plain region ranges :,;," -in width from a few kilometers near its northern end to .12Ir11e nearl)' a thousand kilometers in the vicinity of the Missis-,:r::"'l'~ ... -I~,..-sippi River. The great width near the Mississippi reflects :;:·. the effect of a major downwarped zone in the Earth's .. '-~.;. crust that extends from the Gulf of Mexico to about the ll'.,"' connuence of the Mississippi and Ohio Rivers (fig. 29). This area is referred to as the Mississippi embayment. _ ~-:~ The topography of the region ranges from exten-flJ,.;,-':.. sive, flat, coastal swamps and marshes l to 2 m above sea I::_,;_~ level to rolling uplands, I 00 to 250 m above sea level, along the inner margin of the region. -:._: . 1 ":\-~·. The region is underlain by unconsolidated sedi-lt'· 1 ~ -· ments that consist principally of sand. silt, and clay y~: transported by streams from the adjoining uplands. r.:'fr,-These sediments, which range in age from Jurassic to the 1.-,u,'.J\i .. _,... present, range in thickness from less than a meter near the :~: inner edge of the region to more than 12.000 min south- l !ii.~.~-~~;,_,~-ern Louisiana. The greatest thicknesses are along the 111 ~-seaward edge of the region and along the axis of the Jr,..._ Mississippi embayment. The sedimerits were deposited I_·· on floodplains and as deltas where streams reached the I~;-coast and, during different invasions of the region by the c~t sea, were reworked by waves and ocean currents. Thus, ~----the sediments are complexly interbedded to the extent ~~f that most of the named geologic units into which they ·,i.l-.,.. have been divided contain layers of the different types of 1 ~ sediment that uhderlie the region. These named geologic ,;.,t{t-_•/ units (or formations) dip toward the coast or toward the 1}1_;r_· __ ,, axis of the Mississippi embayment, with the resul.t that ~~..;...-those that crop out at the surface form a series of bands ,g( roughly parallel to the coast or to the axis of the em bay-s:: ment (fig. 41 ). The oldest formations crop oui along the l~-_t-f .. ___ r_· inner margin of the region, and the youngest crop out in ~1!~ the coastal area. @~, ·. \Vithin any formation the coarsest grained mate- 1,, ·:_'·:' · nals (sand, at places interbedded with thin gravel layers) o/ tend to be most abundant near source areas. Clay and silt * layers become thicker and more numerous downdip (fig. •. lfi:.__41). le:i· Although sand. silt. and clav. as noted above. are ~_::~~-the principal types o_f material u~derlying the Atlantic , ~';'j!~ and Gulf Coastal Plain. there are also a small amount of :+~-- 52 Cround-Water Regions of the United States --·----------·--··--·------------------. gravel interbedded with the sand, a few beds composed of mollusk shells, and a small amount of limestone present in the regiori. The most important limestone is the semi-consolidated Castle Hayne Limestone of Eocene age which underlies an area of about 26.000 km2 in eastern North Carolina, is more than 200 m thick in much of the area, and is the most productive aquifer in North Caro-lina. A soft, clayey limestone (the chalk of the Selma Group) of Late Cretaceous age underlies parts of eastern Mississippi and western Alabama. but instead of being an aquifer it is an important confining bed . From the standpoint of well yields and ground-water use, the Atlantic and Gulf Coastal Plain is one of the most important regions in the country. Recharge to the ground-water system occurs in the interstrcam areas. both where sand layers crop out and by percolation downward across the interbedded clay and silt layers. Discharge from the system occurs by seepage to streams, estuaries, and the ocean. Movement of water from recharge areas to discharge areas is controlled, as in all ground-water systems. by hydraulic gradients, but in this region the pattern of movement is complicated by down-dip thickening of clay which hampers upward discharge. As a result, movement down the dip of the permeable layers becomes increasingly slow with increasing distance from the outcrop areaS. This causes many flow lines to converge on the discharge areas located on major streams near the do\Vndip part of outcrop areas. These areas of concentrated ground-water discharge are referred to a_s "artesian-water gaps" by LeGrand and Pettyjohn ( I 981 ). Figure 42 illustrates the effect of an artesian-water gap on heads and flow lines in an ideal situation. Wells that yield moderate to large quantities of water can be constructed almost anywhere in the region. Because most of the aquifers consist of unconsolidated sand, wells require screens; where the sand is fine-grained and well sorted, the common practice is to surround the screens with a coarse sand or gravel envel~pe. Withdrawals near the outcrop areas of aquifers are . rather quickly balanced by increases in recharge and ( or) reductions in natural discharge. Withdrawals at signifi- ---.. ,,,,.::,'' ~~:.,____:__: , .. ....._ .. ~ ' ' .... ,· - l~~I Fresh water j~j Salty water ' Figure 41. Topographic and geologic features of the Gulf Coastal Plain. Major stream ---, Outcrop area · 8re8 2 / . -----'--'~-:-. nd s·,\t) . . bed \cla'{ a .~?Z: confln,n9 _ .. -• --· . ~~ .. PLAN VIEW DIAGRAM Figure 42. Concentration of ground-water discharge near the downdip part of outcrop areas. cant distances downdip do not appreciably affect condi-tions in the outcrop area and thus must be partly or largely supplied from water in storage in the aquifers and confining beds. The reduction of storage in an aquifer in the vicin-ity of a pumping well is reflected in a decline in ground-water levels and is necessary in order to establish a hydraulic gradient toward the well. If withdrawals are continued for long periods in areas underlain by thick sequences of unconsolidated deposits, such as the Atlan-tic and Gulf Coastal Plain, the lowered ground-water levels in the aquifer may result ind rainage of water from layers of silt and clay. The depletion of storage in fine-grained beds results in subsidence of the land surface. Subsidence in parts of the Houston area totaled about 9 m as of 1978. Subsidence near pumping centers in the Atlantic Coastal Plain has not yet been confirmed but is believed to be occurring. though at a slower rate than along the Texas Gulf Coast. The depletion of storage in confining beds is per-manent. and subsidence of the land surface that results from such depletion is also permanent. On the other Atlantic and Gulf Coastal Plain 53 ~i,~.-.f ~ ... ;ot.' .--~ I ~ .. ~.,., Jft)/}1' I-~?~• .. . . {fa_ '.ftl.}t ,-.,--.. o ri-'"1 r1 ,~.;~.> Lli)6i§E(C li~tC2ffri1eff1rlL§ =;\ff ,J I .. ,t·'., •. ·.: •.. ·i'.·~.-~.: __ ·,,.·· (?'~ r" 1r", n r -1 t"_· tTi1 = 'f\ DV, I"?, f:-('Jj r-~ ,_,:; ·-.::.).:u QJJ\Yj,i l:\1,/.:i V, 01~¼,,..,Ll .... ~-:::· --· t , .. ,1e, ~--0 n r~~ a,~;;~, -.. ...f'.J '""'l 1 ;_!/ (2 ,)-n-,ri''(.C•t T/'Y\111. fT'CJ:i.· ,1 \~ .'(· \j \.J . • .. REF. 18 l,N,•~:~. \', (c',:, Ll tUl I Li\?;.-..:,,_ Li\~ Ii ';; , Ll l:: ~ ~ -~;.ltr o ~ J rt ~ 1 flftl _1:"o~·[mi ~~~~~;tl~a , -· . -, YO i~;. '. . ~ ·· .. _. ,. ,... ·•,c;;,_,:·:'·:::;-c ·.S:c,o, , ■wt: -·: -_ -,---•--.---. .-'. .:~_}_:_;_·_.~,: <,. , ~,:Ji.·. ·. ._.:,:\_ .. \_:~.'.:'". ~ :._;~~'::..:.7'-,:.::3 '· .",(.'··· . · · . .,.. · , ...,., -..... :·. '·?~~-.. .-..... - ' .: . : -... ~~•·r • I•-• lflt tl,S. GEOi..OGtCAl SURVEY iEfC.: ,,.i"l;t,,-V/ATER RESOIJR.CES ir--JVEST1GAT!01'1S lijt;··-c,?cr\i··F1LE REt;ORT 80-l;-4 wi~~-. 114~- ,~~ .-tt r, . , .. i'i! ~·· r· Prep2reci in cooperation with the Nonn C2ro!i.1a Depar:ment of Natural R,·sour.::es 2nd Co.:imu;-iity Developme;-it ll' H" - ... ~ " 0 ,., u ;~ ,., "' u u OJ' 61' F.XPL/\IJ/\TION u ~ 0 '"' _, 0 FK"t:·-:r·ru,coloo\a·· fofmotion tf]Ui-L.:.'. .. ·.: volcnl ( sands ond clop I ~[w Triassic ,ans !somJslone nnd conqlome1otes) ~ /-<;,~-~ V 'Ir-J \r 1. .J "-·,:Z -l .)'\" ,:;-.1,.,~v .._\...,'\ V ., ~\1,,., \::.t" ,,,," ®"' f~~~C"/1~ ~ -~t" V D<."''-" \,/'\=.~ P,~ .. ~~ G1or11l1c f-:' ~~~~1 M cl omor phoH d s e di men Io r y k,.,:--.:' ond volcanic rocks ([[[[[J Gneiss and SC hist r-:;-:-~ Moslly micoceous ~ond gneiss SC his r ,,. ,.. --'i . ' ., Georgia-Pacific Corp. Hardwood Srnmill NCO 000 813 592 n• '<\ L>-c· '\·GL~ ~ -'--~..:.-~. , . if,i:,;,.-. . l~--~~\.·rfock Units and Aquifers ~;t,u;: ·the Coastal Plain :ii'fG!••.1 rn . ~-;iit' l i,'K'~~~ . . tffr" .. :;( -r ~;;:r',r--· t~?'~\~;;;_·· The Coastal Plain of North Carolina is ~~ ~nderlain by sedimentary rocks that were ll!Nt,;r; deposited in w_ater in ,several different layers ie,~s"'~ which geologists re,er to as formations. I . ,;cZ~ Formations are commonly given names for ~s::.·. places near which they are exposed at the land !&~.~:i: surface, for ease in re~erring to them in ~l::i':··-geologic literature. IS::: Rock layers are normally given names by ;,;:-··· geologists if they have a distinct composition rn~!.~-.c or, if of variable composition, inciude materials I"' ~t. deposited during a particular segment of ~~:. geologic time. Named rock units may or may q~;:( not coincide with hydrologic units so that in tyc~!fi'.:•·~-ground-water reports some aquifers may be It;:· referred to_ by the formal geologic names used ,'., by geologists, such as the Castle Ha,,ne -r:ra"ii/::._ Lir11estone and Yorklov,in Formation, and r-.. ,~ ~ I. "-Z..--ethers may be given more informal names, il;:,,.. such as the."Upper aquifer", "Surficial aquifer" i~-~~. or "post-Miocene deposits." The name ml§}B;<. "Surficial _aquifer" indicates the aquifer i_n an_y l f&P area that 1s closest to land surface and •nus 1s ,iJ;., .. clearly identifiable, regardless of any other ,, .. J! .. ir . names that may have been assigned lo that ruo-~ /;!i~-~1 : rock unit It:;; . Nr:n·g;ologists concerned both with ground- ~'.\·( watar problems and w_ilh ground-water studies 1:.1•w'.\*-,,_.·: .. 1n the Coastal Plain are probably con- 1,1,ft.,. ~ .... -.. /' I/~.~~ ~~" it:: .1!~ ,~~---~. - I. ;'.f.';f,;;·· .r~. -r-:;:,; !iill'¾1'",:. ~-Is~ lij,J~-~::· ..--;;:t;.' .•• l~t i;?,- Geologic age Pleistocene Pliocene Miocene Oligocer:e Eocene Paleoce:;e C;et2.csous Formation or geologic na.me P le i.s tocene deposits Cree.tan Forroa tion Yorkto·.~•n Form2tion Pun;o River Formation Belc;~2.de Fol."":.1atio::! River 3end Formation Castle Hayne Limestone Be2.ufort Forrn2.tion Peedee For.nation Black Creek Formaticn 11 Tuscaloos2.11 :'or~1.s.tion fused by the different named applied to tc,e different hycrologic units. The following chart was prepared in an eifort to elimina.te some of this confusion. We should note, however, that in preparing the chart we have neither tried to include all formation names nor been overly concerned with the relative geologic age of the formations. The names used in the last tv,0 columns can be confusing to the extent that al! units are reierred to as "aquifers." Confining beds composed of clay occur in all of the formations and in the formations of Cretaceous age clay comprises about half of the total thickness. The two most important aquifers in the Coastal Plain are the upper aquifer and the limestone aquifer. Recharge of the ground- water system is fro.m precipitation on the land surfar,e. Therefore, the surficial aquifer has the largest yield in terms of rate per unit area (for example, gallons per minute per square mile). The upper equifer is also most subject to pollution from land-surface waste disposal. The limestone aquifer is the most productive aquifer in North Carolina in terms of yie!ds of individual wells. Wells capable of yielding more than 1000 gal/min can readily be developed in this aquifer. l\2mes used in some Simpliest useful ground-·,.,·2. ter ·reoorts hydrologic names Post-Miocene deposits Up;ier aquifer Yorktown 2quifer C2.stle Hayne c.,~;Jife!' I Li:nes tone 2.quife~ Be2u fort 2ql!ifer Lc-..:er 2.quifer Cretaceot.:.s cqi..:if'er ~ I! 22 !t~·t ~- BIi' ;,,,-;. < ·. ~7;'.,· l !~;f;. ,,..,..; ,?..~ .. ",I, ... , ,. ' ~·~r:-The complex inlerlcying: o~ lhe ·sedi:11ents · ·•· •;; ~~derlyir,g the Co2s:aI Pi21n ,s shown ,n the P.following cross section. It 1•:ill also be observed ~lfrorn the cross section that the rock layers (end- ~" ;,: ;. ... 23 formations) underlying the Co2st2I Plain di;:, lowerd the coast 21 a r2te of about 15 ft./mi. /\s a resul!, each form2tion occurs 2t a gre2ter depth below !2nd surlace tow2rd the coast. · -••oc ·. Stream ,CASTLE \ I Clay Recharge a re o HAYNE AQUIFER 24 ~ h l.2.2.2} S e 11 s Limestone the deepest aquifers occurs only in the central part of the interstre2rn recharge areas. This is an important point relative io waste disposal, in that if pollution of the deeper aquifers is to be avoided, waste disposal sites should be located as close as possible to perennial streams. Prior to the construction of drainage ditches into the central part of the interstream areas, the water table reached ihe land surface in these areas dt.!ring the fa!I, winter, and early ,spring recharge season. As a result, water was ponded on the surface· for periods of several months each year in high-level swamps reierred to as pocosins. Two region·a1 aspects of the Coastal Plain are of primary importance from the stcndpoint o: ground-water occurrence and availability. The iirst is the nature of the surficial materials, which controls the recharge to the ground-wa;er system. The second ·,s the geolog·,c con- dilions ihat control the occurrence of aquifers and confining beds. ' 1 r ' i •11,.,,. w:-~¢.;._,. ·~:'' -~~•j: l ~lg~.-'.~t· ' $i;if,,::. ~~ ........ :;r a.: ,, ,Ji'!,1./:c~-' ..... ~-1151~,, :.; . ~•;:;.:1r~-:zt." .. · l ,..;/L~, ""'''l' .;,~ rroH'It nf'ttttUJt'TDWWSTWi zszm:HMF&il -111 . jf.t::' l~l.L~YDRAULIC CONDUCTIVITY AND TRANSMISSIVITY VALUES ,,.,, t(.f.•,., . ~"ff!=.'-"-FOR TYPICAL NORTH CAROLINA ROCKS AND AQUIFERS Ir ;;;..~-c•·· . · t• ·r•"': ~~ .. : <;-It" • .,,... ~C- -•.,j~._-· ~ Hydraulic Conductlvlly of Selected Rocks Hydraulic conductivity {rounded values) . •· (/Vdoy) [(0.11//diiy)/IP] (mi,\era/d.11y) nPT1f3fC'2::i?xt lf.i,;7 Maler/al i:f. ;, -z:. .j.:,l,,, Coarse sand . . . . . . . . . . . . . . . . . . . . . . . 200 1500 60 ;>,o:, " 10 .z:. l",j,. Medium sand . . . . .. .. .. .. . . . . . . .. .. 130 1000 40 'J-,69 x 10 _4 ,7'. Silt ................................ 1 5 0.2 3.53 x ,o_:::. '•!\-Clay............................... 0.001 0.01 0.0004 3.53 ;< •0 _1 '£:7/,\,, Limestone (Castle Hayne) . . . . . . . . . . 300 2000 80 I • c,c.. x ,c I~:; Saprolite . . . .. .. . . . .. . . .. .. . . .. .. .. . 5 50 2 1, '1-'J. x ,o-!- ' Granite and gneiss .. .. . . .. .. ..... . . . 5 50 2 I.-,-. , ,c·3 1-:,: Slate . . . . . . . .. . . .. .. . . . . . . . . . . . . . . . 3 25 1 1, 06 ,: 10-~ lr,i,-\t:_ .· Hydraulic conductivity replaces the term "field coefficient of permeability" and should be used when . ."r-referring to the water-transmitting characteristic of material in quantitative terms. It is still permissible IU~~trnfer in qualitative terms to "permeable" and "impermeable" material. \"( -{i;i\l\s:,· Average Values of Hydraulic Conductivity, Thickness, and Transmlsalvlty M1:<.i::.· · for Selected Aquifers In North Carolina .::. Hydr.11u/lc Conducllvlly Thlckneu Tr.11nsmh1lv!ty ~ti}~,;-·~--Aquifer. Cm. I~ EC... {fl.ld.11y) (It.) (l!l./d11y) 11fj:,;~t-Yor~~own deposits 1.'I-+ x. 10 ·\_ 50 20 1000 :.ij,.Yorktown Formation I, r '1 x 10 50 40 2000 •£:"~Castle Hayne Limestone 1.06 ;< ,o-~ 300 100 30000 l~.~ .. Cretaceous deposits + .or, K ,t>-_3 20 • 200 4000 ~~ Saprolite I . 1 'I Ji Io 5 50 250 l ;r;}!ranite and gneiss . I , 7-7 J,( , o -,, 5 200 1000 r Transmissivity replaces the term "coefficient of transmissibility" because, by convention, an aquifer · rti::::•;::::i"' ;s• :• ':• ;: ::: , ":::~:,,:::m," ts of gmo"d-wa t ec hydco 1 ogy ~~with reference to conditions in North Carolina; U.S. Geological Survey ~rater-Resources ~nvestigations Report 80-44) 11·, H YD"R. ,~ u l-1 L. C....c"-Jt:,t..,;e_.--:-1 v 1 ;-y -...:.r, . .,-(\L ____ r"T ?o,Sc,v./rT l;~~D~...Jvt:: 14-S, c,>--.) r • O~-. -X __ _ ,1 __ . Dr, ·1 86+= :sc.c.jD1' Y 1i--· 1:· i .. } .... I N FT 3,5 3 -4 X IQ J\J .5E C. GEOLOGie'1'1\1ap OF NORTH CAROLINA ' . . ' :, ' . ' ' -------------·-·· ------ . -------.· --~·--:-~ 1985 Scale 1:500,000 1 inch equals approximately 8 miles ... "' I mmrme ft illi1fFtFW ___ II . <·>t~S:i;;:;-~:~:;· i\~ -:~.:: · ~-:., \.r;;·:;{(1:tf ~~1f 11~'.'.}:_.j):=J: · . xt,t~f iilf :,,:, --· '0 Op ! . Tp I l:W ,,,; ;;: I I >tq,?;J;j Tpy COAST AL PLAIN . ' ·:~' ·-. -· .... :_:~· QUATERNARY !:. SURFICIAL DEPOSITS: UNDi&ioEO :...:·sand: ~lay, gravel. and peat depo-, sited in mari:1e, fllivial, eolian, and lacustrine environments. Quaternary deposits not shown at .:iltitudes greater than approximately 25 feet above mean sea level (Suffolk Scarp, in part) TERTIARY· PINEHURST FORMATION -Sand. medium-to coarse-grained, cross-bedding and rhythmic bands of clayey sand common. unconsolidated TERRACE DEPOSITS AND UPLAND SEDIMENT -Gravel, clayey sand. and sand, minor iron-oxide cen:iented sandstone WACCAMAW FORMATION -Fossiliferous sand with silt and clay, bluish-gray to tan, loosely consolidated. Straddles Pleistocene-Pliocene boundary YORKTOWN FORMATION AND DUPLiN FORMATION. UNDIVIDED Yorktown Formation: Fossiliferous clay with varying amounts of fine-grained sand, bluish gray, shell material commonly concentrated in lenses; mainly in area north of Neuse River Duplin Formation: Shelly, medium-to coarse-grained sand. sandy marl. and limestone, bluish gray; mainly in area south of Neuse River ~~ BELGRADE FORMATION. UNDIVIDED Pollocksville Member: Oyster-shell mounds in tan to orange sand matrix. indurated locally Haywood Landing Member: Fossiliferous clayey sand. gray to brown. Members grade into each other laterally ~~1\ RIVER BEND FORMATION -Limestone. calcarenite overlain by and intercalated with indurated, sandy, molluscan-mold limestone 1111:r&'~ 11·11 lilil ,,,,! I I Tee [ Km, CASTLE HAYNE FORMATION Spring Garden Member: Molluscan-mold limestone, indurated, very sandy. Grades downward into a calcareous sand and laterally into Comfort Member Comfort Member and New Hanover Member, undivided Comfort Member: Bryozoan-echinoid skeletal limestone. locally dolomitized, solution cavities common New Hanover Member: Phosphate-pebble conglomerate, micritic. th in; restricted to basal part of Castle Hayne Formation in southeast-ern counties BEAUFORT FORMATION, UNDIVIDED Unnamed upper member: Sand and silty clay, glauconitic, fossiliferous, and locally calcareous Jericho Run Member: Siliceous mudstone with sandstone lenses, thin bedded; basal phosphatic pebble conglomerate CRETA.CEOUS PEEDEE FORMATION -Sand, clayey sand. and clay. greenish gray to olive black, massive, glauconitic, locally fossiliferous and calcareous. Patches of sandy molluscan-mold limestone in upper part BLACK CREEK FORMATION -Clay, gray to black. lignitic; contains thin beds and laminae of fine-grained micaceous sand and th·rck lenses of cross-bedded sand. Glauconitic, fossiliferous clayey sand lenses in upper part MIDDENDORF FORMATION..:... Sand. sandstone. and mudstone. gray to pale gray with an orange cast, mottled; clay balls and iron-cemented concretions common, beds laterally discontinous, cross-bedding common CAPE FEAR FORMATION -Sandstone and sandy mudstone. ye\!owish gray to bluish gray, mottled red to yellowish orange, indurated, graded and laterally continuous bedding, blocky clay, faint cross-bedding. feld-spar and mica common t. Aldri st C n, 2, Bart\ B a' C · 3. B!ac! a: u 4. Buth. ir; ., 5. Buci, 0- ti E 6. Deb l ' ti 7. Drul ~- C 8. Farr c i 9. Ful!i I 10. FulL 11. Fuli 12. Fu\' 13. Full 14. Fu! 15: Gk ' ,. ,• /I ,. !: l.' I i, I i/ ., ·, I SOIL SURVEY OF REF. 20 ashington County, North Carolina I I I United States Department of Agriculture Soil Conservation Service in cooperation with North Carolina Agricultural Research Service North Carolina Agricultural Extension Service Washington County Board of Commissioners, and North Carolina Department of Natural Resources and Community Development nsnszrmrw SFSTZTCTW mrvrcrrr:ar:r PT 7 i:W? I This soil is well suited to pasture forage such as fescue and Ladino clover. I This soil is poorly suited to most urban and recreation uses because of wetness. The dominant native trees are sweetgum, red maple, I yellow-poplar, baldcypress, willow oak, and water oak. The understory includes mainly sweetbay, southern bayberry, giant cane, pawpaw, fetterbush lyonia, inkberry, and greenbrier. Wetness is the main limitation to I woodland use and management. This Fortescue soil is in capability subclass Vlw and woodland group 2w. · I Hy-Hyde silt loam. This is a nearly level, very poorly drained soil in the Blacklands. The mapped areas are irregular in shape and range from 10 to 500 acres in I size. · Typically, the surface layer is 17 inches thick. It is very dark gray silt loam in the upper part and very dark grayish brown silt loam in the lower part. The subsoil is II 41 inches thick. The upper part is grayish brown silt II loam, the middle part is dark grayish brown and light brownish gray silty clay loam, and the lower part is light brownish gray silt loam. The underlying material to a II depth of 85 inches is greenish gray silt loam in the upper II part and stratified sand, loamy sand, and sandy loam in the lower part. Included in mapping are small areas of Cape Fear, II Portsmouth, and Roper soils that are common in D adjacent areas. Most of the included soils are near the outer edge of the map unit. g The organic matter content in the surface layer of the Hyde soil is high. Permeability is moderately slow. The soil is extremely acid to strongly acid throughout, except where limed. The seasonal high water table is at or near n the surface. This soil is subject to rare flooding. Most of the acreage of this soil is cultivated. The rest is mainly pasture and woodland. 0 If drained, this soil is well suited to most locally grown crops. Corn and soybeans are the dominant crops. Wetness is the main limitation. Minimum tillage, cover crops, and grasses and legumes in the cropping system lihelp maintain tilth and crop production. Spring tillage and ufall harvest can be delayed because of wetness. Lack of suitable outlets and moderately slow permeability are limitations to the installation of drainage systems. B This soil is well suited to pasture forage such as escue and Ladino clover. This soil is poorly suited to most urban and recreation uses. Wetness is the main limitation to those uses. l The dominant native trees are loblolly pine, red maple, sh, sweetgum, elm, water oak, and willow oak. The understory includes mainly American holly, sweetbay, I ourwood, reeds, and southern wax myrtle. Wetness is he main limitation to woodland use and management. This Hyde soil is in capability subclass II lw and woodland group 1 w. I I Soil survey Me-Muckalee loam. This is a nearly level, poorly drained soil on flood plains of small_ streams that flow into Albemarle Sound and the Roanoke River. The mapped areas are oblong and range from _5 to 30 acres in size. Typically, the surface layer is dark gray loam 20 inches thick. The underlying material to a depth of 64 inches is gray sandy loam in the upper part, dark gray sandy loam in the middle part, and gray, stratified sand and loamy sand in the lower part. Included in mapping are small areas of Dorovan mucky silt loam. The organic matter content of the surface layer of the Muckalee soil is medium. Permeability is moderate. The soil ranges from strongly acid to slightly acid in the upper part and medium acid to neutral in the lower part .. The seasonal high water table is within 1 /2 foot to 1 1 /2 feet of the surface. This soil is frequently flooded for brief periods. Most of the acreage of this soil is woodland. This soil is poorly suited to crop production. Flooding and wetness are the main limitations to this use. Lack of suitable outlets is a limitation to the installation of drainage systems. The soil is well suited to pasture forage such as fescue and Ladino clover, if it is drained and protected from flooding. This soil is poorly suited to recreation uses. Flooding and wetness limit those uses. Frequent flooding is a severe limitation to urban uses. The dominant native trees are baldcypress, pond pine, red maple, green ash, hickory, sweetgum, swamp tupelo, elm, yellow-poplar, river birch, water oak, and willow oak. The understory includes mainly cedar, American holly, sweetbay, sourwood, reeds, and waxmyrtle. Wetness and flooding are the main limitations to woodland use and management. This Muckalee soil is in capability subclass Vw and woodland group 2w. Pe-Pettigrew rauck. This is a nearly level, very poorly drained soil in the Blacklands. The mapped areas are irregular in shape and range from 1 0 to 500 acres in size. Typically, the surface layer is black muck 15 inches thick. The upper part of the underlying mineral soil is very dark grayish brown mucky clay loam 5 inches thick. The subsoil is 30 inches thick. It is very dark gray clay loam in the upper part and dark gray clay in the middle and lower parts. The underlying material to a depth of 7 4 inches is greenish gray and dark gree1:ish gray, stratified sandy clay loam, sandy loam, and coarse sanci. Included in mapping are small areas of Roper, Hyde, Wasda, Cape Fear, and Belhaven soils that are common in adjacent areas. Most of the included soils are near the outer edge of the map unit. Permeability is moderately slow to moderately rapid in the organic layer of Pettigrew muck, and ii is slow lo very slow in the upper mineral layers. The shrink-swell rsa J: i 1 '• I 20 I and stumps in the organic layers have to be removed ~ efore cultivation. Spring tillage and fall harvest may be elayed because of wetness. During spring planting, soil lowing can occur. Conservation practices such as lf inimum tillage, the use of field borders, and the use of indbreaks reduce the chance of soil blowing. This soil is poorly suited to most urban and recreation uses. Wetness, flooding, and low strength are limitations io those uses. The dominant native trees are red maple, sweetgum, aldcypress, and blackgum. The understory includes mainly inkberry, fetterbush lyonia, huckleberry, ( eenbrier, waxmyrtle, and switchcane. Wetness and coding are the main limitations to woodland use and anagement. This Scuppernong soil is in capability subclass Vllw gind woodland group 4w. TaB-Tarboro sand, 0 to 3 percent slopes. This is a somewhat excessively drained soil in the northern part of IJhe county. It is on low, broad ridges commonly adjacent IJo Albemarle Sound and the Roanoke River. The mapped areas are irregular in shape and range from 10 ~ o 250 acres in size. Typically, the surface layer is 12 inches thick. It is dark rayish brown sand in the upper part and brown sand in the lower part. The underlying material to a depth of 60 IE. ches is sand. It is brownish yellow in the upper part, ellowish brown in the middle part, and yellow in the wer part. Below that to a depth of 99 inches is pale brown sand. ' Included in mapping are Bojac and Conetoe soils, hich are common in adjacent ~apped areas. Most of he included soils are near the outer edge of the map unit. Small areas of soils that are not as well drained as • his soil may occur in small depressions within the unit. The surface layer of Tarboro sand is low in organic matter content. Permeability is rapid, and available water lapacity is low. This soil ranges from strongly acid to lightly acid, except where limed. Most of the acreage of this soil is cultivated. The rest is mainly woodland. This soil is suited to a few crops, such as peach l rchards, peanuts, and soybeans. It does not have ufficient moisture for most crops during the growing season. Leaching of plant nutrients, soil blowing, and low - vailable water capacity are the main limitations. Blowing and can damage young plants. Minimum tillage, crop esidue, the use of windbreaks, and close-growing grasses and legumes in the cropping system help control ■oil blowing and conserve moisture. Split applications of ltrtilizers, particularly nitrogen, are needed. This soil is suited to pasture forage such a.s Coastal bermudagrass - nd bahiagrass. This soil is well suited to most urban uses. The thick andy material provides good support for most .structures. The unprotected sandy surface, however, is lubject to soil blowing and is draughty when rainfall is I Soil survey limited. Seepage from septic tank filter field lines is sometimes a problem. This soil is suited to recreation uses; however, the sandy surface layer is sometimes a limitation. The dominant native trees are loblolly pine, longleaf pine, sweetgum, southern red oak, blackjack oak, white oak, post oak, and red maple. The understory includes mainly dogwood, sassafras, and American holly. The low available water capacity is the main limitation to woodland use and management. This Tarboro soil is in capability subclass Ills and woodland group 4s. To-Tomotley fine sandy loam. This is a nearly level, poorly drained soil. It is on slightly elevated areas in the Blacklands and in depressions near small streams that flow into Albemarle Sound and the Roanoke River. The mapped areas are irregular in shape and range from 10 to 150 acres in size. Typically, the surface layer is dark gray fine sandy loam 6 inches thick. The subsurface layer is light gray fine sandy loam 5 inches thick. The subsoil is 53 inches thick. It is light gray sandy loarri in the upper part, gray and light olive gray clay loam in the middle part, and gray sandy loam in the lower part. The underlying material to a depth of 80 inches is gray stratified sandy loam, loamy sand, and sand. Included in mapping are small areas of Augusta, Roanoke, and Portsmouth soils that are common in adjacent mapped areas. Most of the included soils are near the outer edge of the unit. In the Tomotley soil, the organic matter content is medium. Permeability is moderate to moderately slow. The soil ranges from extremely acid to strongly acid in the upper part, except where limed. Below a depth of about 50 inches, it ranges from extremely acid to medium acid. The seasonal high water table is at or near the surface. This soil is subject to rare flooding. Most of the acreage of this soil is cultivated. The rest is mainly pasture or woodland. The soil is well suited to most locally grown crops. Corn and soybeans are the dominant crops. Wetness is the main limitation to cultivation. Winter cover crops, minimum tillage, and crop residue help maintain tilth and production. Conservation practices such as no-till planting, the use of field borders, and the use of crop rotations that include close-growing crops also help conserve soil and water. The soil is well suited to pasture forage. This soil is poorly suited to most urban and recreation uses because of wetness. The dominant native trees are loblolly pine, sweetgum, red maple, yellow-poplar, willow oak, water oak, black cherry, and American beech. The major understory includes dogwood, sourwood, sweetbay, and sassafras, along with a variety of briers and reeds. Wetness is the main limitation to woodland use and management. This Tomotley soil is in capability subclass lllw and woodland group 2w. I I I I I Ii! l R lli __ ·. ,;w I ;_ Washington County, North Carolina i· I .Pl_,~ ;.,.. -~ . tt~1-( subangular blocky structure; very friable; strongly II" 1; acid; abrupt smooth boundary. 11~\g :ucg-36 to 72 inches; grayish brown (2.SY 5/2) sand; r ll~~-· single grained; loose; slightly acid. 11, .. ,. ail?' The surface mineral layers range from 20 to 35 inches dL'12! in thickness. The underlying organic horizons range from I":1.ff 1 0 to 30 inches in thickness. The soil is extremely acid !~ or strongly acid throughout the surface mineral layers DI~_ and the buried organic layers. The und~rlying ~ineral ,;,:'m horizons of some pedons range to medIu_m acid or •• ~·slightly acid. D~~-The Ap or A1 horizon has hue of 10YR or SY, value of ,, .. •· 2 or 3, and chroma of 0 to 2. ·, -~-The IIOa horizon has hue of 2.SYR or SY, value of 2 ~!~ or 3, and chroma of 0 to 4. It is well decomposed 0-~ organic material. Fiber content is less than 1 percent ~-\~\ d t.\;~ rubbe . . . . rt.':'lfo The IICg horizons are grayish or greenish sand, loamy /1\~j~ sand, or sandy loam. IJffi,-11~ Hyde series ~'To•ttl-: r.: ,~ · The Hyde series consists of very poorly drained soils I :~f_ ;.,that formed in unconsolidated loamy fluvial and marine 'i/f.." deposits. Slope ranges from 0 to 2 percent. Wi~,ir,, Typical pedon of Hyde silt loam, approximately 0.6 f;.i:¼. · mile east of Wenona lookout tower, 0.1 mile east of 1~_1.~_ intersection of State Road 1128 and State Road 1129, ,;il 200 feet north of State Road 1129 in the third "cut" east [4fa:~! "A Canal": lt,f'Ap-0 to 12 inches; very dark gray (10YR 3/1) silt loam; (~'.t;} moderate medium granular structure; very friable; f ~.::C: · common fine roots and crop residue; few fine clean l[~\t~ sand grains; very strongly acid; clear smooth ,~,;;,. boundary. lli[;~tiJ. 12-12 to 17 inches; very dark grayish brown (1 OYA f:';,.)'.;Ji1,. 3/2) silt loam; moderate fine subangular blocky and IL. >iii;,(-granular structure; very friable; common fine roots ~~.,.. .. and old root channels; few fine pores; few fine [~,; °fi,j;--. flakes of mica; extremely acid; clear irregular .. ,.'£1'.'R' boundary. I'~· .B1-17 to 21 inches; grayish brown (10YR 5/2) silt , .,i4i;:;_ loam; moderate fine subangular blocky structure; · ,,;~1,:-, firm; slightly sticky, slightly plastic; common fine and lflf-[; medium roots and pores; common very fine flakes of ,;:; , mica; extremely acid; clear wavy boundary. ltG· B21tg-21 to 37 inches; dark grayish brown (1 OYA 4/2) l'½"f£ silty clay loam; few medium distinct strong brown l~f;° (7 .SYR 5/6) mottles on faces of peds and along root f:,;/,\ channels; moderate angular and subangular blocky II.\~:;,~;,_-'--structure; very firm; sticky, plastic; common fine and l.'t~.ifJ'." · medium roots and pores; common very fine flakes of l ~i-mica; extremely acid; gradual wavy boundary. ,w,:'.:~~22tg-37 to 45 inches; light brownish gray (2.SY 6/2) ,, -~· silty clay loam; common medium distinct strong .. ::'~:" brown (7.SYR 5/6) mottles on faces of peds and ,; ~f-F . i,}fl ·•~,Jf,~ -~!"·,, i, ..... ·. ~t;; 51 along root channels; moderate fine angular and subangular blocky structure; very firm; slightly sticky, slightly plastic; common fine roots and pores; common very fine flakes of mica; extremely acid; gradual wavy boundary. B3g-45 to 58 inches; light brownish gray (2.SY 6/2) silt loam; common fine distinct brownish yellow mottles on faces of peds and along root channels; moderate fine subangular blocky structure; friable; slightly sticky, slightly plastic; common very fine flakes of mica; extremely acid; abrupt smooth boundary. C1g-58 to 67 inches; greenish gray (SG 5/1) silt loam, with pockets of very fine sand; massive; friable; common very fine flakes of mica; extremely acid; gradual wavy boundary. IIC2g-67 to 85 inches; greenish gray (SG 5/1) stratified sand, loamy sand, and sandy loam; massive; very friable; common very fine flakes of mica; extremely acid. Hyde soils have a loamy Bt horizon 20 to 40 inches thick. The soil ranges from extremely acid to strongly acid, except in limed areas. Few to common flakes of mica occur throughout the profile. The Al horizon has hue of 1 OYA or 2.SY, value of 2 or 3, and chroma of 0 to 2. The B1 horizon has hue of 1DYR or 2.SY, value of 4 to 6, and chroma of 1 or 2. It is silt loam or loam. The B2tg horizon has hue of 1 OYA or SY, value of 4 to 6, and chroma of 1 or 2. Mottles in shades of brown or red are common in the B2tg horizon. Texture is silty clay loam or clay loam. The B3 horizon is similar in color to the B2tg horizon. It ranges from silt loam to silty clay or sandy loam. The C horizon is greenish gray, grayish brown, or light gray or mottled gray, brown, and reddish brown. It is stratified sand, sandy loam, or loamy sand. Muckalee series The Muckalee series consists of poorly drained soils that formed in loamy fluvial sediments. Slope is less than 2 percent. Typical pedon of Muckalee loam, approximately 2 miles southeast of Plymouth; 150 feet west of State Road 1181 on State Road 1115 and 1 00 feet northeast of bridge on State Road 1115: A11-0 to 9 inches; dark gray (10YR 4/1) loam; weak medium granular structure; very friable; slightly sticky, slightly plastic; common fine roots; strongly acid; clear wavy boundary. A12-9 to 20 inches; dark gray (1DYR 4/1) loam; few fine distinct yellowish brown mottles around root channels; massive; friable; sticky, plastic; common fine roots; strongly acid; gradual wavy boundary. C1g-20 to 32 inches; gray (SY 5/1) sandy loam; common medium distinct dark greenish gray (SGY 52 a D 4/1) mottles; massive; friable; slightly sticky, slightly plastic; few fine flakes of mica; slightly acid; gradual wavy boundary. C2g-32 to 42 inches; dark gray (SY 4/1) sandy loam; D massive; friable; few fine flakes of mica; slightly acid; gradual wavy boundary. C3g-42 to 64 inches; gray (10YR 5/1) stratified sand and loamy sand; massive; very friable; common n partially decomposed roots and fibers; few fine flakes of mica; slightly acid. The A horizon ranges from strongly acid to slightly 0 acid. The C horizon ranges from medium acid to neutral. There are few to common flakes of mica throughout the profile. · The A1 horizon has hue of 10YR or 2.5Y, value of 3 to D 5, and chroma of 1 or 2. . The C horizon has hue of 1 0YR or SY, value of 4 to 6, and chroma of 1 or 2. It is sandy loam or loamy sand. II Some pedons have strata of sandy clay loam, sand, or II loamy sand. The Muckalee series has siliceous mineralogy. Because the Muckalee soils in this survey area have I mixed mineralogy, they are considered a taxadjunct to the series. They are similar in use, management, and behavior, however, to the Muckalee series. I Pettigrew series The Pettigrew series consists of very poorly drained soils that formed in clayey marine deposits under I extremely wet conditions. Typical pedon of Pettigrew muck, approximately 1.5 miles northwest of Lake Phelps and 0.5 mile southeast I of First Colony Farms grain elevators, 0.4 mile south of main east-west canal and 100 feet east of main north- south canal in 10th cut: I Oap-0 to 7 inches; black (N2/0, broken face and rubbed) muck; moderate medium granular structure; very friable; common fine roots and crop residue; few small pieces of charcoal; strongly acid; clear I smooth boundary. Oa2-7 to 15 inches; black (SYR 2/1, broken face and rubbed) muck; moderate medium subangular blocky I structure; friable; slightly sticky and pastelike; common fine and medium roots; few pieces of charcoal and few pockets of ash; few vertical cracks up to 1 / 4 inch wide; extremely acid; gradual smooth boundary. I A 1-15 to 20 inches; very dark grayish brown (1 0YR 3/2) mucky clay loam; weak fine subangular blocky structure; very friable; slightly sticky, slightly plastic; I common fine to medium roots and fibers; extremely acid; gradual smooth boundary. B1g-20 to 26 inches; very dark gray (10YR 3/1) clay loam; weak medium subangular blocky structure; I friable; sticky, plastic; common fine to medium roots I and fibers; extremely acid; gradual smooth boundary. B2g-26 to 36 inches; dark gray (10YR 4/1) clay; weak fine subangular blocky structure; very firm; very sticky, very plastic; common fine to medium roots and fibers; strongly acid; gradual smooth boundary. B3g-36 to 50 inches; dark gray (N4/0) clay; massive; ·,y, very firm; very sticky, very plastic; common fine to -..,.,. medium roots and fibers; strongly acid; clear smooth _w .' boundary. Jj", ,: IICg-50 to 74 inches; greenish gray (5G 5/1) and dark '..\: \ greenish gray (5G 4/1) stratified sandy clay loam, :~J,:; sandy loam, and coarse sand; massive; friable or • .i ·· loose; sandy clay loam and clay loam is slightly ",al), sticky, slightly plastic; common fine flakes of mica; -~--~' slightly acid. ·illi:i~'\ 1.Y;, Thickness of the muck and clayey materials over •~', unconforming sediments ranges from 40 to more than 60 ./~~•· inches. Reaction ranges from strongly acid to extremely "f,i-# acid In the upper part of the control section and medium ·-ff'ti acid to mildly alkaline in the lower part and in the C · ¼~.ii horizon. Few to common fine flakes of mica are in the ·:1:.,·•1 lower part of the B and in the C horizons. J ' The Oap or Oa1 horizon has hue of 5YR or 2.5Y, ·~;: value of 2 or 3, and chroma of 0 or 2. In drained areas, it ~~ has weak to moderate medium granular structure. The .J}j Oa2 horizon has hue of 2.5YR to 2.5Y, value of 2 or 3, ':i-jji/ and chroma of 0 to 4. In drained areas, it has weak to :jf moderate medium subangular blocky structure. The ~~t unrubbed fib_er content ranges from 2 to 20 percent, and i.ii the rubbed fiber content ranges from 0 to 4 percent. :~, Charcoal fragments and pockets of ash are few to ·~fi common in the organic horizons of some pedons. '.~'&'. The A 1 horizon has hue of 1 0YR or SY, value of 3 or ··· .. ~· 4, and chroma of 0 to 2. It is loam, clay loam, mucky clay loam, silty clay loam, or sandy clay loam that is 8 to ;;.t 20 percent organic matter. Some pedons do not have an 11() A 1 horizon. · .i.:tfi The B horizon has hue of 1 0YR or SY, value of 3 to 6, '~ ,_ and chroma of o to 2. It is clay loam, clay, or silty clay. .-.:[ef_,_X~ Few to common mottles of higher chroma are iri some ::i pedons. ~ The C horizon is grayish or greenish, stratified sandy _;! and loamy sediments. .;.;;.: j Ponzer series The Ponzer series consists of very poorly drained organic soils. The organic layers are 16 to 51 inches thick over loamy textured marine and fluvial sediments. Slope ranges from 0 to 2 percent. Typical pedon of Ponzer muck, approximately 0. 7 mile northwest of intersection of State Road 1126 and State Road 1183, 2. 7 miles northeast of State Road 1126 on dirt road; 50 feet southwest of dirt road: · ;~-r: _;-1.V:(I ·t -~fli1 "<;~ ~,~,~ j, '1~·-. ·i:; "J -~_fl __ ·' Oa1-0 to 13 inches; black (10YR 2/1, broken face and Ill:~~ rubbed) muck; less than 5 percent fibers, less than t;:_ ,71.! ;· #g a 56 d Scuppernong series I The Scuppernong series consists of very poorly drained organic soils. The organic layers are 16 to 51 inches thick over loamy sediments that are high in silt n and organic matter and overlie sand. Slope ranges from 0 to 1 percent. · Typical pedon of Scuppernong muck, approximately 1.5 miles south of State Road 1126 on State Road 1183, U 500 feet east of State Road 1183: Oap-0 to 5 inches; black (5YR 2/ 1, broken face and rubbed) muck; less than 1 percent fiber unrubbed D and rubbed; moderate fine and medium granular structure; very friable; common fine and large roots and fragments of wood; strongly acid; abrupt smooth boundary. DOa2-5 to 9 inches; dark reddish brown (5YR 2/2, · broken face and rubbed) muck; less than 1 percent fiber unrubbed and rubbed; massive parting to weak fine angular blocky structure; friable; slightly sticky II and pastelike; common fine, medium, and large II roots and fragments of wood; few fine pieces of charcoal; extremely acid; clear smooth boundary. Oa3-9 to 20 inches; dark reddish brown (5YR 3/2, II broken face and rubbed) muck; about 5 percent II fibers, less than 1 percent rubbed; massive;' friable; slightly sticky and pastelike; common medium and I large roots and fragments of wood; few medium pieces of charcoal; extremely acid; gradual wavy boundary. Oa4-20 to 28 inches; dark reddish brown (5YR 3/3, II broken face and rubbed) muck; about 15 percent II · fibers, 2 percent rubbed; massive; friable; slightly sticky and pastelike; common medium and large roots and fragments of wood; few medium pieces of I charcoal; extremely acid; clear wavy boundary. IIC1g-28 to 45 inches; dark greenish gray (5GY 4/1) mucky silt loam; massive; slightly sticky; common fine streaks and pockets of light gray very fine sand I and silt; extremely acid; clear smooth boundary. IIIC2g-45 to 48 inches; light gray (10YR 7/1) sand; single grained; loose; few medium flakes of mica; extremely acid; gradual wavy boundary. I IIIC3g-48 to 72 inches; dark greenish gray (5GY 4/1) sand; single grained; loose; few medium flakes of mica; extremely acid. I Thickness of the organic material ranges from 16 to 51 inches. The organic horizons are extremely acid (in 0.01 molar of calcium chloride) except where the surface I layer has been limed. The mineral horizons range from extremely acid to neutral. Logs, stumps, and fragments of wood occupy 0 to 15 percent of the upper organic horizons in cultivated or pastured areas and 10 to 35 I percent in undrained_ areas. A few (0 to 2 percent) pieces of charcoal and pockets of ash occur in the organic layers. Flakes of mica are few to common in the 1 mineral horizons of most pedons. I The Oa1 or Oap horizon has hue of 5YR or 10YR, value of 2 or 3, and chroma of 0 to 3. In cultivated or , pastured areas, it has weak to moderate fine and ,Yi'f;._ .. medium granular structure. Structure in the Oa2 horizon •I, -'" occurs only in drained areas that are cultivated. The :1"' '' structure is massive but parts to fine and medium angular blocky. - The Oa2 horizon and underlying organic tiers have tiu· of 2.5YR or 5YR, value of 2 or 3, and chroma of 2 or 4. -l The lower tiers of organic matter are pastelike, have a _ , greasy feel, and are massive under natural, wet _., 'i\i ~ conditions. If the soil is drained and cultivated, its ·:'.,,_" .!_,. 1 structure changes upon aeration. Excessive drying ~ ~· ,, causes shrinkage and the formation of hard angular ;~ , blocky peds. These peds dry irreversibly. Fiber content is ~11~ 1 highest in the lower tier. It ranges from 10 to 50 percent.~~ , unrubbed and less than 10 percent rubbed. ;,})!ii · The IIC1g horizon has hue of 5GY, 5G, or SY, value of ~t'IJ~_/' 3 to 5, and chroma of 1 or 2. It is silt loam or silty clay .. ~~~: j loam and contains 1 0 to 20 percent organic matter J¥1i . throughout. '1U\. The IIICg horizons have hue of 10YR or 5Y, value of 6.~' or 8, and chroma of 1 or 2 and range to greenish gray' or' :1;1 dark greenish gray. They are sand or loamy sand. --111 ' Tarboro series ·;~ . ~,,1,'>i The Tarboro series consists of somewhat excessively -~~ ,,,; drained soils that formed in sandy fluvial sediments. _ ·ii·"·' Slope ranges from 0 to 3 percent. ~f' ., Typical pedon of Tarboro sand, Oto 3 percent slopes, .1. ~\ approximately 0.5 mile east of intersection of State Road \ ,:. 1315 and N.C. Highway 32, and 250 feet south of 1, :, Albemarle Sound in the woods: ·:~~ A 11-0 to 3 inches; dark grayish brown (1 0YR 4/2) sand; weak fine granular structure; very friable; many fine and medium roots; many clean sand grains; strongly acid; clear smooth boundary. A 12-3 to 12 inches; brown (1 0YR 4/3) sand; weak fine granular structure; very friable; common fine to coarse roots; few organic stains on sand grains; few very fine opaque grains; strongly acid; clear wavy boundary. C1-12 to 31 inches; brownish yellow (10YR 6/6) sand; single grained; loose; few fine to coarse roots; few fine flakes of mica; few very fine opaque grains; strongly acid; gradual wavy boundary. C2-31 to 52 inches; yellowish brown (1 0YR 5/6) sand; single grained; loose; few medium and large roots; few fine flakes of mica; _few very fine opaque grains; strongly acid; clear wavy boundary. C3-52 to 60 inches; yellow (1 0YR 7 /8) sand; single grained; loose; few fine flakes of mica; few very fine opaque grains; medium acid; clear smooth boundary. C4-60 to 99 inches; pale brown (1 0YR 6/3) sand; single grained; loose; few fine flakes of mica; few very fine opaque grains; strongly acid. !~1 ,,~ .~ ;iii;~' :;t,,, 'ir.1 -~.,,,..,· ~ .,ii/mt '· '" "· 3, ~ ·v , 1~ ~~ 11 /~ ~ 'i. -,. ·,'/Ii·•, :~: □ D 0 0 D 0 D u I I I I I U S DEPARTMENT OF AGRICULTURE . ~OIL CONSERVATION SERVICE Georgia-Pacific Corp. Hardwood Sawmill NCO 000 813 592 . ,-]W~ !-... ·, .. , / 780000 r .. FEET >,, -~~ e ~ ~ ~ {i ~ • ,: : =··--. ~ : . ,· .. ~\~~-,\ • ~L • ~G~~ REF. 21 NORTH CAROLINA DEPARTMENT OF CONSERVATION AND DEVELOPMENT WILLIAM P. SAUNDERS, Director Division of Mineral Resources JASPER L. STUCKEY, State Geologist Bulletin Number 73 GEOLOGY AND GROUND-WATER RESOURCES IN THE GREENVILLE AREA, NORTH CAROLINA By PHILIP M. BROWN Geologist, Geological Survey United States Department of the Interior PREPARED COOPERATIVELY BY THE GEOLOGICAL SURVEY UNITED STATES DEPARTMENT OF THE INTERIOR 1959 I• '.~.~!l:.!t{ir: ir-m~, .... ,. ~;~he?:·. t~(~1~~ · ·~ · , . Jil§F/f~'Lf-Z" . Martin County f/~,\~•:r,,-, (Area 481 square miles, population 27,938) n:.,,f,r,I~~,;·,· Martin County, elongated in an east-west direc-ij ' 'thin, lies approximately in the geographical center of P., , ;f the Greenville area. The county is bounded by Pitt, :;;; ;~:'. Bertie, Washington, Beaufort, Edgecombe, and Hali-rY~~if.j fax Counties._ Williamston,. the county seat and ~-"~" largest town m the county, 1s located on the banks l ;;it~!: of the Roanoke River, which forms the northern ,.'fi:.'i!tfftiounclary of the county. Other population c.enters in-~l;,4';;~".t,' elude Bear Grass, Hamilton, Jamesville, Oak City, I " .,,.-:-and Robersonville. . J,F, ... The entire county is drained by the Roanoke River \;;~.~:' -and several of its small tributaries. A high escarp-w.'· ~-.:,. I,~.·::-''· ment broken by numerous low swampy ~reas extends _,.,;::-· along the Roanoke River for most of its length. f~r'· The county is largely agricultural, tobacco being I .,;,,., -. the chief crop. A large pulp mill and a chemical ~-:r· manufacturing plant are the major industries in the tifmJK·~ county. ii;;f.{;;.. Geology.-Surficial clay, sand, and gravel of Quat-li!ilf,0·, . ernary age occur as a thin layer over the entire coun-~11:: ty. Along the Roanoke River and its tributaries this f6il~--material is as much as 40 feet thick; in the inter-e:r·: stream areas it is rarely more than 15 feet thick. if;/.;.: . The surficial deposits are underlain by the York-1,f-town formation of late Miocene ~ge, which consi~ts .~"'·· of blue clay, marl, and sand. The 1. orktown format10n t.l'!~ff;c',. is exposed intermittently along the Roanoke River, l ~irii,:-where the stream has cut down through overlying ~~: material, and is exposed in many shallow marl pits :/-1:<l'f'.'i' in the interstream areas. The formation is common-l~""'i,::.~_ly le~s than 80 to 100 feet thick throughout the ,;t;i,'ii~_,county. Jl¾lf'.'· The Castle Hayne limestone of Eocene age under-llf.~_c lies the Yorktown formation in the eastern part of I*~;,_ . Martin County. Wells east of Jamesville and Smith-ti:i:'c/.' wick obtain water from the Castle Hayne limestone F-§~-;:'"" for~ation which in this part of the Greenville area 11f(~, consists of a very hard shell-limestone .. Wells at , .'./' Williamston and Bear Grass do not encounter the ~,~;;;.':;formation, indicating that the formation pinches out ' ~.•:;~_;' al~ng a line west of Jan_ies~ille and Smit~wick. Total 1'1!,'-· thickness of the format10n m the county 1s unknown. t.~ p..;;~~.-Glauconitic sands and shell beds of the Beaufort l~.'..: .. i_c-.. c: formation of Paleocene age underlie the eastern and i'f·: central thirds of the county. The formation, confin-l?t'-ed to the subsurface, has not been recognized west I~ of Williamston and Bear Grass. Total thickness of :f,i_: _ this unit in a well at Williamston was 27 feet, where 'f!p.! the top of the unit was 59 feet below sea level. Its l•~:i, 70 ~fr-. ~-.... t:f.··· l~t::,:, ~l?f· ~i~ ii:'Eiii Slnli1i- total thickness and its depth below sea level would be expected to increase in an easterly direction. The Upper Cretaceous Pedee and Black Creek for-mations, composed of dark-colored lenticular sands and clays, underlie. the central and eastern sections of Martin County. The western extent of these for-mations has not been determined. It is probable that marine sediments of these two formations interfinger with deltaic sediments of comparable age in the west-ern part of the county. The Peedee formation at Williamston is 129 feet thick and the top of the for-mation is 86 feet below sea level. The Black Creek formation is 259 feet thick at Williamston . The basal Upper Cretaceous unit, the Tuscaloosa formation, underlies the Peedee and Black Creek for-mations in the eastern and central parts of Martin County. In western Martin County this formation lies unconformably beneath Paleocene and Miocene sediments. The Tuscaloosa formation, composed of light-colored lenticular clays and arkosic sands, lies within 40 to 50 feet of the land surface in the west-ern part of the county and is buried progressively deeper in an easterly direction. Estimated thickness of the formation in the eastern part of the county is about 400 feet. Sediments of Early Cretaceous age probably un-derlie the Tuscaloosa formation in the eastern and central parts of Martin County, whereas in the western part of the county the formation is underlain by crystalline rocks. Ground water.-All public and private water sup-plies in Martin County are obtained from wells. Mar-tin County is favorably situated as to ground-water supply. Several millions of gallons per day of ground water may be obtained at any one place in the coun-ty. Larg-diameter gravel-wall wells will yield as much as 1,000 gpm in most localities. Surficial sands and gravels of Quaternary age and near-surface sand and shell beds of the Yorktown formation yield 2 to 10 gpm. Rural supplies in the county are obtained largely from dug or driven wells that tap the aquifers of Miocene or Quaternary age. Small-diameter jetted wells in eastern and central Martin County draw water from sand lenses and shell beds of Miocene age, limestone of Eocene age, and greensand of Paleocene age at depths ranging from GO to 200 feet. These wells, either open-end or single-screen, yield as much as 50 gpm. Jetted wells in western Martin County obtain water from sand lenses and shell beds of Miocene age and from sands of Cretaceous age. These wells, generally less than 400 feet deep, yield from 10 to 300 gpm. REF. 22 SIMULATION OF GROUND-WATER FLOW IN THE COASTAL PLAIN AQUIFER SYSTEM OF NORTH CAROLINA U.S. GEOLOGICAL SURVEY Open-File Report 90-372 SIMUIATION OF GROUND-WATER FLOW IN THE COASTAL PIAIN AQUIFER SYSTEM OF NORTH CAROLINA By G.L. Giese, J.L. Eimers, and R.W. Coble U.S. GEOLOGICAL SURVEY Open-File Report 90-372 f Raleigh, North Carolina 1991 nm riz-zrnrtttam58Di f aquifers they overlie. Thus, aquifer Al is the lowermost aquifer and the confining unit overlying it is CUl. These designations are referred to frequently in this report. Selected hydrogeologic sections were adopted from Winner and Coble (1989) to show the distribution of aquifers and confining units throughout the North Carolina Coastal Plain (figs. 5 through 9). The idealized sections show the thickening, thinning, and pinch-outs typical of these hydrogeologic units in the study area. Confining units are considered to terminate at the limit of the underlying aquifer. These relations are built into the modeling process, and the reader is referred to Winner and Coble (1989) for detailed geologic and hydrologic descriptions. Brief descriptions of each hydrogeologic unit are presented in this section. Surficial Aquifer (AlO) The surficial aquifer (AlO) overlies all of the North Carolina Coastal Plain (fig. 1) and consists. of fine sand, silt, clay, shell, and peat beds. Scattered deposits of coarser-grained sediments in the unit occur in relict beach ridges or in alluvium. Throughout the western and central parts of the Coastal Plain, the thickness of the surficial aquifer ranges from a few feet to about 30 ft (feet); however, the aquifer thickens eastward and is more than 200 ft thick in the vicinity of the Outer Banks. The sediments of the surficial aquifer are primarily of post-Yorktown age, but are not / restricted to a single geologic unit in terms of age or lithology (Winner and Coble, 1989). The surficial aquifer (AlO) directly overlies most of the confined aquifers at one place or another_ and exchanges Water with them either directly or through an intervening confining bed. The surficial aquifer receives direct recharge from precipitation and is the source of water for the deeper confined aquifers and base flow to streams. The amount of recharge from precipitation varies areally depending on the clay content of the soils. from about 12 to 20 in/yr, Winner and Coble (1989) estimated the average horizontal hydraulic conductivity of the surficial aquifer to be 29 ft/d (feet per day). A more detailed description of movement of water Within the surficial aquifer is given in the section entitled "Model Input.11 14 ~ r~·,i1, . • •'\!J:' .. ~-1'•,• I ·;; ... ,..·.n·· ·•if1 (•·'':- i'f.'.l''.~-~- '. '·• .f;;, •~--:,~.''.·. I":_ -~'""- 1·"' ;..;.._ 1· I a -~ .. I··,::· ,. 'l;...i;; . - I,, ... ir~ l '.!'1)( !:°!.' . . ' I~-·~;·· ;l,.._ IW•:.~_- •--· ·1-· ' =•::/ -, ... t·.-:·-. :---· I"',::·. ... I- I-.•· ,. ·, .1-J .. ; ,. , •'•· ., ;:,:_· Yorktown Aquifer (A9) and Overlying Confining Unit (CU9) The Yorktown aquifer (A9), is equated with the older beds of the Pliocene Yorktown Formation of Clark and others (1912) and extends throughout the northern half of the Coastal Plain (fig. 10) from the Fall Line, where it overlies crystalline rocks similar to those in the Piedmont, eastward to beyond the coast. The Yorktown aquifer is largely composed of fine sand, silty and clayey sand, and sand with shells and shell beds, with some limestone and coarse sand beds also present. In the western Coastal Plain, the aquifer is relatively thin, less than 20 ft thick in many places, and has been cut into or eroded away by the larger streams flowing across the area. In Dare County, the Yorktown aquifer attains its maximum thickness of over 300 ft. The Yorktown aquifer (A9) does not extend into the southern half of the Coastal Plain, except for a small area in Robeson County (fig. 10) which is the largest of a number of outliers shown by Brown and others (1972, pl. 21). Figure 10 also shows the areal extent of aquifers that underlie the Yorktown aquifer. The surficial aquifer (Al0) overlies the Yorktown aquifer everywhere. The estimated horizontal hydraulic conductivity of the Yorktown aquifer (A9) ranges from 19 to 33 ft/d and averages about 21 ft/d, based on aquifer tests and lithologic-and geophysical-log data from 52 wells and test holes ,.. (Winner and Coble, 1989). The Yorktown confining unit (CU9) overlying the Yorktown aquifer is comprised of the youngest clay beds of the Yorktown Formation in most places, but locally may include clay beds of Pleistocene or Holocene age. Its thickness averages about 25 ft, ranging from less than 10 up to 50 ft thick. It is composed largely of clay and sandy clay that locally includes beds of fine sand or shell. The Yorktown confining unit generally is considered to extend only as far as the Yorktown.aquifer, even though stratigraphically equivalent beds may continue beyond the aquifer limits . 20 Pungo River Aquifer {AP) and Overlying Confining Unit {CUB) The Pungo River aquifer (A8) consists of the permeable part of the Pungo River. Formation of lower and middle Miocene age, described in detail by Kimrey (1965). The Pungo River aquifer is composed of fine to medium marine sands with considerable phosphate content. Average estimated horizontal hydraulic conductivity based on analysis of geophysical logs is 33 ft/d, according to Winner and Coble (1989). Shells and other fossils are present throughout the aquifer; occasionally, beds of limestone and coarse sand are found. The Pungo River aquifer (AB) is thinnest near its western and northern limits, where its thickness averages about 15 ft. The aquifer dips eastward and thickens to more than 200 ft in the vicinity of the Outer Banks where the top is more than 700 ft below sea level. The aquifer is overlain everywhere by aquifers A9 or AlO (fig. 11), except where it is exposed in an open-pit phosphate mine in Beaufort County. The Pungo River aquifer is underlain everywhere by the Castle Hayne aquifer (A7). The Pungo River confining unit (CUB) is formed by the upper clay beds of the Pungo River Formation and contiguous clays of the lowermost Yorktown Formation. The confining unit ranges in thickness from less than 10 ft near the western margin to about 150 ft beneath Currituck County, with an ave,age ,thickness of nearly 55 ft. For most of the area, the confining unit is f composed of nearly uniform clay containing less than 10 percent sand. Castle Hayne Aquifer {A7) and Overlying Confining Unit (CU7) The Castle Hayne aquifer (A7) is delineated as those calcareous sediments of Eocene age that are equated with the Castle Hayne Limestone and the Trent Formation of former usage of Clark and others (1912). Also included in this aquifer are rocks of Oligocene age, now designated River Bend Formation, overlying the Castle Hayne (Brown and others, 1972), which are lithologically identical and hydraulically connected to the Castle Hayne Limestone. The basal part of the aquifer may include older contiguous permeable units in local areas. The areal extent of this aquifer is shown in figure 12, which also shows the extent of overlying aquifers. 22 36" 79• 78" . IT JrntflcPJ51157PfflifMt:M FffiiP§'f2frmr:rree:m&xw:rrrtt1t1t-ce"-@ Georgia-Pacific Corp. Hardwood Sawmill NCD 000 813 592 77• 76" j ELL I , DARE ('--. ·7 \ \ \ I ·; ;;c_ ""' r~,.,.. ) .. / ·r·"' ✓' ~/RJCH..;,,,~:.,,·/ HOKE icuMSERW<o\ .Jso~ '\ · · "' /7 35• . . ( ..... _ \..'" ·, , -~-/ ----<;'.__'v' ___ / 1\--~\\ (., <v,~ ! 34• 33• ~~ j_ ./'' i:;.,,. --·-....__ +· C'l-,~O , COI..UMBUS / I_.;;.$ ?,.,:""'· . ...,..--· Ii , f BRUNSWlCI< "' . --•---"--,;cl SO MltES e-------~ SOKILOl.4ETERS EXPLANATION !lill-'...,! CASI'LE HAYNE AQUIFER NOT PRFSENT 212.._ LIMIT AND DESIGNATION OF AQUIFER DIRECTLY OVERLYING CASTLE HAYNE AQUIFER AND ITS CONFINING UNIT AIO Surficial aquifer A9 Yorktown aquifer A8 Pungo River aquifer Figure 12.--Areal extent of the Castle Hayne aquifer (A7) and overlying aquifers (modified from Winner and Coble, 1989). 24 ' i I r I i i I = m:rtttt ·w ftitNWW77tICW17$$! 5 pr Limes·tone may occur as shell limestone, dolomitic limestone, and sandy .limestone ranging from loosely consolidated to hard and recrystallized. Along the western margin, the aquifer occurs near land surface from New Hanover County to Craven County. Eastward, the aquifer thickens to more than 950 ft in Carteret County and to nearly 1,200 ft beneath Cape Hatteras (Brown, 1958, fig. 4). In the area north of Albemarle Sound, limestone beds are thin to nonexistent 1 and the sediments contain more clay. The thickness of the unit averages about maximum of 115 50 ft between Bertie and Currituck Counties but reaches a ft in Currituck County. The Castle Hayne aquifer (A7) is the most productiv~ aquifer in North Carolina due to its thickness and high percentage of permeable limestone and sand. On the basis of aquifer tests and lithologic and geophysical log data, the hydraulic conductivity of the Castle Hayne aquifer ranges from about 15 ft/d, where it is composed of fine sand, to about 200 ft/d where the bulk of the aquifer is porous limestone. The thickness of the Castle Hayne confining unit (CU7) averages only about 10 ft; it exceeds 25 ft only i.n Gates County along the Virginia border, in eastern Pamlico and Carteret Counties, and in two small areas along the western limit of the Castle Hayne aquifer (A7). The confining unit is composed of beds of clay, sandy clay, and clay with sandy streaks that· are part of the Pungo River Formation, the Yorktown Formation, or younger clays. The confining unit is missing in several stream valleys south of Craven County and in two areas in the northeastern Coastal Plain. In addition to being thinner than most of the other confining units, the Castle Hayne confining unit contains more sand; thus, it is relatively, permeable and allows significant vertical leakage between the Castle Hayne and overlying aquifer_s. The Castle Hayne aquifer (A7) and confining unit (CU7) are directly overlain by the Pungo River aquifer (A8) throughout most of its northern and eastern area (fig. 12), whereas to the south, the Castle Hayne is overlain by the Yorktown and surficial aquifers (A9 and AlO). The Castle Hayne is directly underlain by the Beaufort aquifer (A6) and confining unit (CU6) northeast of Jones and Onslow Counties and by the Peedee aquifer (AS) and confining unit (CUS) south of these counties (fig. 13). 25 I I I' i' I I' i l \ I I 1:/. Is*.;: __ -· ?' . ,·,: I 1: ..... ,~ i::'.~- 1\1.~:.: ... .. I,· .. -. -··· .;:; ~ ·ltl!'z-.'.. ; : ,. ~· Ill';'~-.. . ' ~7;--·"·• l "':i;':'.:• -··'. ~-.,,., i,-~_-~.-u- ·--· ti··· 11: t-· 11 ' As previously mentioned, the model assumes all flow in aquifers to be horizontal and all flow in confining units to be vertical. It was recognized 1 however, that in many places within zones designated as aquifer material, the thickness of clay is significant, and this clay often functions as an impediment to vertical flow. A more realistic simulation of the flow system was obtained by incorporating the effects of clay within aquifers into the leakance terms. Accordingly, total effective thickness (b) values for each confining unit were generated (figs. 35-43) which represented the sum of (1). effective confining unit thickness, (2) one-half the thickness of clay beds in the aquifer above the confining unit, and (3) one-half the thickness of clay beds in the aquifer below the confining unit. At some locations shown in figures 35-43 where the confining unit is designated as not present (particularly in stream valleys), the clay within aquifers concept was used to assign an effective clay thickness for modeling purposes . Initial values for K , representing the vertical hydraulic conductivity V of confining unit material, were based on appraisals of confining unit effectiveness derived from geophysical logs, differences in head between aquifers above and below the confining unit, and chemical analyses, using as a guideline values of vertical hydraulic conductivity for various materials given by from 1 x Morris and Johnson .3 10 ft/day to 4 x (1967, table -6 10 ft/day. 6). These initial values ranged At many locations, two or more confining units need to be considered for modeling purposes as occurring between two non-sequential aquifers (case A in fig. 44). For example, the lower Cape Fear aquifer (A2) may be present and directly above it the lower and upper Cape Fear confining unit (CU2), and the Black Creek aquifer (A4) may be present. The upper Cape Fear aquifer (A3) and upper Cape Fear confining unit (CU3) are missing in this example. In this situation the lower Cape Fear confining unit (CU2) is considered as being composed of two confining units: half of the effective thickness belonging to the lower Cape Fear confining unit (CU2) and the other half belonging to the upper Cape Fear confining unit (CU3), even though the upper Cape Fear confining unit (CU3) is not present. In general, the confining ·unit is divided into N + 1 equal parts, where N is the number of missing aquifers. Although the transmissivity of the missing aquifers is 60 ~;,',.1, . -' ·~i .. ; .~ . . I~ \ ., / .. ~ ;t .. lol1,{ ~,.. ❖.,;' i!<1,, • A•- \,'::}: . . ,· lt~t·,:- ~~-- REF. 23 .. f,:: .-;··_;:..:c.··: :~-:·'-;· - . GEOLOGY AND GROUND-WATER· ... _,._._,,_.,.-RESOURCES '·· · · ··.. of the ·•-~- ~---..... i . .:. .:.. ·: .• :. SlViNQ'uARTER ARE( NORTH CAROLINA ... -•' ·-. . . ·· .. , •-,,: Division of Ground Water · GROUND-WATER BULLETIN NUMBER 4 NORTH CAROiINA DEPARTMENT ()F WATER RESOURCES \ RALEIGH· .. 1964 ~~}T!':,, •~1:•·· ;·,;r:~t,g~-:~J~J~t!t~r~0J~?f'fi,: , ,.·,:•·· ·: -.< ..... ,,·.:··?;~:~~: .?\·_{)_;/.;:~-:---\ .. :.? Collection of G. C. Niche Ison GEOLOGY AND GROUND-WATER RESOURCES of the SWANQUARTER AREA, NORTH CAROLINA BY PERRY F. NELSON GROUND-WATER BULLETIN NUMBER 4 NORTH CAROLINA DEPARTMENT OF WATER RESOURCES w ALTER E. FULLER, Director DIVISION OF GROUND WATER HARRY M. PEEK, Chu;/ RALEIGH 1964 II fflt"":'WM WASHINGTON COUNTY Area 336 Square Miles Population 13,488 (1960) Washington County is bounded on the north by Albemarle Sound, on the east by Tyrrell County, on the south by Hyde and Beaufort Counties, and on the west by Martin· County. The county occupies a part of the low, flat plain of the Pamlico ter-race, with the exception of the western border which is under-lain by an older marine terrace and is slightly higher in eleva-tion than the rest of the county. Principal Aquifers Washington County is underlain by a thick section of sedi-mentary deposits ranging in age from Cretaceous to Recent, and consisting mainly of sand, clay, marl and limestone. Only the formations of Eocene age and younger are consid.ered to be sources of fresh water supply in the county, as the depth of the older formations and the relatively high mineral content of the water preclude their use as sources of supply. The beds of sand and marl of Paleocene age that underlie the Eocene rocks in Washington County may constitute a source of fresh water sup-ply in the southwestern part of the county. However, data con-cerning the geologic and hydrologic nature of the formation and the quality of the water contained are not adequate to determine the potential of the formation as an aquifer. A cross section of the formations generally penetrated by water wells in the county is shown in figure 20. Tlie Castle Hayne aquifer is highly productive and the prin-cipal source of water supply in western Washington County. The aquifer consists predominantly of porous and permeable limestone and lies at a depth ranging from about 120 feet in the western part of the county to 400 feet in the eastern part (fig. 20). Yields of several hundred gpm are obtained from wells of four to eight inches in diameter that penetrate only 15 to 30 feet of the aquifer. Considerably higher yields can probably be obtained from wells that penetrate a greater thickness of the formation. The Yorktown aquifer, comprising all the confined water-bearing beds above the Castle Hayne aquifer, has been devel-oped extensively as sources of domestic water supply in the county, and is the chief source of supply in the eastern part 53 ~l~fff1 ·::: .. . : .:.,. :_. · ... -~·\./~:-: l ~;Y.«':;,~cc_:,;;.,.,,r,:,._,,,ij,:~,'.W, ··1 r:~~--t~~~rt~tr:::?1r1;;mrit:?~} . t ~,~.er,:.~--:-:_.~ .. ~_.;.-;<::t.':??~r:¾z;-:·~\:<:• ' : ,~:--. ~ .. .-: ... •:-,_-:;.: ... J:>~•~:·,: }l ... _~· . .::-:.· :·-,:•::::~ :.::-; .:.:~:·-::.; --.1.--.:;: ~- :, ·. ,:;: f:; ,; ;-:: ir l~f~'.li-,S.·,, 1;: ;;t,~ ''1'!,:,;:,~.:. · , i~~ ·-~:~;£t:IS:.~~ ~\~•;,..;~~ '<:~ ·~· ~ -~~~-x-.~ ,1t--,&-.!.,,t; .,,-v,,. ! ~--!· , .... :.,,,,~ ........ -~~~r.<1~~-r~....,-~ Jal where it is about 300 to 350 feet thick, In this area, the aquifer offers a shallower and less highly mineralized source of water supply thari the Castle Hayne aquifer, Yields from individual wells range from 5 to 60 gallons per minute, A 6-inch well, 135 feet deep at State Prison Unit 019, was pumped at a rate of 60 gallons per minute for 12 hours with 7 feet of drawdown, indicating a specific capacity of 8,5 gallons per minute per foot of drawdown, In the western part of the county, the phosphatic sands in the lower part of the aquifer should provide moderate yields to wells completed at depths of 150 to 200 feet. The non-artesian aquifer yields water to numerous dug or driven wells throughout the county. Wells completed in this aquifer range from 10 to 30 feet in depth and yield from 3 to 20 gallons per minute, Most wells in this aquifer are now being used as supplemental rather than a primary source of supply. Water Levels Water levels in the Castle Hayne and Yorktown aquifers are everywhere within 10 feet of the land surface, Figure 7 shows the configuration of the piezometric surface of the Castle Hayne aquifer in Washington County, In low areas, particularly in the northwestern part of the county, where the elevation of the land surface is less than that of the piezometric surface, flow- ing wells occur, The water table, or upper surface of the non-artesian aquifer, is within a few feet of the land surface, The water table re- sponds rapidly to local variations in the amount and distribu- tion of precipitation, and may during periods of drought fall below the bottom of some sha'llow wells. The· hydrographs in figure 21 show water level variations in selected wells in the county during 1962, Water Quality Ground water in Washington County, although not of uniform quality, is satisfactory for most domestic uses, Water from the Castle Hayne limestone is characteristically hard, may be locally high in iron and may contain objectionable amounts of hydrogen sulfide, The chloride content of water in the Castle Hayne ranges from 10 parts per million in the southern and southwest- ern part of the county to 750 parts per million in the Creswell 56 .. fr:~',:i~'.:...71.0.:'i:/. :-::: ~-~f:.-;/~£Jti~ . I~~-:~~-;~~:~;:!..:~:~ l,;.::~.'.:.'!t~;{+~-;:..,~~Y, ~~~ '':-,:.' -~-• ~ • ',.,_ )-z::i:~_..,,-,,., .. ..1,-t-;,.,.\.~-;.:-,"";,-.:,,1.;:,,.._,;~Mf; • ~lmm;i ~'-.,-~• ,J :1 ~:.-~;~µ:';·{./:t°"T,~ :~::~~-;~;-,.-1~.:t~~11 ~ (.,, i ,i:~~~~~ : r.t!~ ,.:... ~,.. ::~~ i •~~f•,• .. ,,;:~,_:-•,-,,5 ~"'-"-! 'Z • Y-:.,•.-,: -~\-t~~ ~'); i, )~""'r,,,c:• . .,, ·\•,p.:v~,;-...;-::0 it,.,;.;..,_.:~,.,-'\',.-.~, · .•:..." J:<1•..+-J/'-1."'J'j" ~ -~•f?~,. r-4-~~x •~:..'.it,:' ,,..,~ :-~~ ... ._-,;,.: -.;,-,:•~--,~-:~ .. "(,,. ... i;•.;.: ,-.ri'.-.f.\s',1~ l•.r . .:'i-.,.;.'•J" '•~·~ f.. • ,:;~ ,,,,,~,;;,:,,;,-'c,,·,;:.;~,,,,.,:fJ,:-~,,; : , i}( .,"~~'%"'1.;(,"\1;fa}'b.~il:~t ,,.,,,,r);,o;:;,, -if.~~ ?. ':r,:, , .. ,-; ,-~~-/y:;;:~-;. -::~ t>J:::·~:;t.Jtt~ ., -~ ~-"' ~ ~~:~~;·~~~~;~ ~~:~t:fS~l:-~~.. ~""'-_fj:i.,. ~\ "t~i~~;t, ~~tf~-~;.~~fi}S~j:::ft1\1~~~~-· 'w· ~ • ~-•si,/fil_ ! jr};1_~: ~1;,~t}1~}~~~~,~~~~~~/'_'ft-' "~. ll'~~l~ ';"<>•i'" ,,.;-,·,:•.-.·, ~,Ji' Nr'1r"' . iii}; ·ilili ~,,.,, ~'fl< ~ '?•-""il~s~:.r !'.•. ,, ~ ,. . ,,;,~ •, .. .; .. :·_-.,,:,. ,:;.:. ~ ·: ..... '" ..... :~:£~.1{h;:~. ~--.... ~•~~1,1 ... -:,.-r.,-~~--)::rJ:\;;:r;:,£.}!!, -!,.~;~~:j.~:!::.~~~~-3{~~1 . , }?.(. ~~., .,-,, .• I;~~. ----·--·· 1··· I I , l -!!!!!! lllliii:a liiii -- - - -- - - I!!!!!! 18 17 16 15 14 13 12 -~ 'o -~ -~ . ~ . ~ CHOWAN COUN Y -.J__ __ ---1-------1---------lf------l-----\ , _,c./_-_,..,.-+------r \) " o........----0 ::.---• '· ~eEM•R~E • ------~-..1__ ----- Georgia-Pacific Corp. Hardwood Sawmill NCD 000 813 592 .. BEAUFORT COUNTY , ' Figure 19.-Map of Washington County showing location of wells H y __ J _____ ]j_ ' ·- D E ' COUNTY,J ~I • ~ e , ~ p u - 15 b ~. ,., 0 ' ~· " m o-, 0 -- 3 6"00 LEGE N 0 L l:15~ 5-minule quodran9,l1 o,b, etc.• l·minut, quodronQlt O·' 0 Wtll Olld numbu Un1ld1 l•mlnutl ~~JI!~~~~~ r 4 W1Lf9 H 'J K L ,.,,,_,,JeYel-Swanquarter •""' -area showi --ng aquifer use d -an water """"" . l!!!!!!!I ---l!!!l!I 1!!1!11 l!!l!!5' !!!!!I 1111!!1 19 l!!!!!!!!I --- tm71i::,-,rJJi"!'9!i'I:!'.: REF. 24 7 Z-WfffEW RMI • ·rffJ~· ID -~r: t,:. • . 'i'; ·-1,;tf: National Water Summary-North Carolina 329 lt:i,,l~~t¥" tJ.f-· ·-~~.~~~~~ttJr;~~~~~!-i?fJ)~i~~:~~:·\?.1?.:::~ff~?:~-.~ !~~-:::;1~;~1~;~f{~f~:;~¥;~:~~i~-~~3f~;;J~~q;~;~::~--~~i?f~\I{;;;~:: Ei,l,r.· ·· NORTH CAROLINA•'h· ,· ,·· .. •c,·soo·.:.••l""''••"·:..••'''',-:;,,1,,• . .,,.,,.,, .• --,-... ,.·., -~ ... -•. ,, .,, .. ,,,.-. ·se;.-:.· ..• -, . .s\·· ... ~r.?iR,~~~i1£~':~?~~~~,~;~t11~~1t~;;~:2:szfvE :f :,:i~~t~i~~: ~CJ:~r.{ttff:·;,:. Ground water is a vital natural resource in North Caroli-Table 1. Ground-water facts for North Carolina I :,._~~,-na Ground water supplies more than 3.2 million people,or [Withdrawal data rounded to two significant figures and may not add S:::::_,. ab~ut 55 percent of the State's total population. Its economic to totals because of independent rounding. Mgal/d == million ~~t': significance is substantial, particularly in the Coastal Plain gallons per day; gal/d = gallons per day. Source: Solley, Chase, ~,e:;·.....,..·_ province (fig. I), where high-yielding aquifers supply most and Mann, 1983] I~~--municipalities, industri7s, rural ~reas, and livestock. In the _____ P_o_p_u_l_a_ti_o_n_s_e_rv_e_d_b_y_g_ro_u_n_d_w_a_t_e_,,_1_9_8_0 ____ _ -, ·~ ~ ... , Piedmont and Blue Ridge provmces, ground. water serves 3,234 • !f!:' Number (thousands)-- - - - - - ~..::.:...;...._ slightly more than one-half of the 4 million residents (Mann, Percentage of total population _ _ 55 'Y ·1¢.17:.-•, 1978). Besides withdrawals for public supply, the largest From public water-supply systems: I k-;.-ground-water withdrawals in the State are for mining and Number (thousands) -----~-:: . quarrying operations and process water for a number of textile Percentage of total population-:: ,;r~1:-·· and chemical industries'. Withdrawals for irrigation represent From rural self-supplied systems: 474 • 8 . • . Number (thousands) - - - - -•r,;..._;_ a small, but increasing, percentage of total ground-water use, 2,760 47 I Percentage of total population-~:::·. particularly in the Coastal Plain. Ground-water withdrawals ~~-: -for various uses and other related statistics are given in table 1. Freshwater withdrawals, 1980 1-, • . <&~:-:. Surface water and ground water, total (Mgal/d) -8,100 770 JO GENERAL SETTING Groundwateronly(Mgal/d) ..•...... • ~; __ :-_.::._ North Carolina is located in three physiographic prov-Percentage of total-- - - -- - - - - - - Percentage of total excluding withdrawals for 3r··. inces-the Coastal Plain, Piedmont, and Blue Ridge (fig. I). thermoelectric power .. ______ . r .. ~.1, • The Coastal Plain aquifers generally are unconsolidated and 20 I LI~t.,;.. • consist of beds of sand, gravel, and limestone separated by clay or clayey layers and lenses. These strata dip and thicken ,._ i'~ southeastward and together comprise a wedge lying on crystal-f,'.;~·, · line bedrock (fig. I). The Piedmont and Blue Ridge provinces :;tr.;..· are, for the most part, underlain by massive crystalline and 1.-. • -, metamorphic rocks that are covered nearly everywhere by a Jr.~--:, ... · claye~ o 1 r sadnd 1 y 1 r7golith consisting of weathered parent rock ,,._ matena an a uvium. ~~i l•tit;.· ,1;'J,..;:.- '10.1. ,--. t"""!')'. lr_·::~~-- /t£...¢..-Iii~-;. I~-~:"'' t.iJ~ J;,C..-• F':'. i· if{-;.~--. 1::,.-~ ,t··. i~_,~=- -·y- Recharge to the ground-water system in North Carolina is derived from precipitation that fanges from about 44 to 54 inches (in.) in the Piedmont and Coastal Plain provinces and from about 40 to 80 in. in the Blue Ridge province (Eder and others, 1983). The amount of precipitation that recharges the gr0'und-water system averages about 20 percent of annual precipitation (Winner and Simmons, 1977; Daniel and Sharp-less, 1983). Most ground-water recharge moves through shal-low aquifers and discharges to streams; only a small part (less than 1 in. in the·Coastal Plain) recharges deeper aquif~rs. PRINCIPAL AQUIFERS The principal aquifers in North Carolina are the surficial, the Yorktown, the Castle Hayne, and the Creta_ceous located in the Coastal Plain and the crystalline rock aquifer located in the Piedmont and Blue Ridge provinces. These aquifers are described below and in table 2; their areal distribution is shown in figure I. SURFICIAL AQUIFER The surficial aquifer is a near-surface deposit of either marine-terrace sand and clay, or sand dunes. It is a principal aquifer in three areas where it is commonly more than 50 feet (ft) thick-the Sand Hills in the southwestern Coastal Plain, the narrow coastal strip of barrier islands called the Outer Banks, and the easte'rn one-half of the mainland north of Pamlico Sound (fig. !) .. In the Sand Hills, where the aquifer may be more than 250 ft thick, it serves as a source for public supplies and irrigation for numerous golf courses (North Carolina Department of Natural Resources and Community Development, 1979). Water from this aquifer in the Sand Category of use Public-supply withdrawals: Ground water (Mgal/d)--- - - Percentage of total ground water-Percentage of total public supply-Per capita (gal/d) --- - Rural-supply withdrawals: Domestic: Ground water (Mgal/d)- Percentage of total ground water -Percentage of total rural domestic Per capita (gaJ/d) - - - - - - -Livestock: Ground water (Mgal/d)-- - - - Percentage of total ground water -Percentage of total livestock - - Industrial self-supplied withdrawals: Ground water (Mgal/d)-- - - - Percentage of total ground water-Percentage of total industrial self-supplied: Including withdrawals for thermoelectric power Excluding withdrawals for thermoelectric power Irrigation withdrawals: Ground water (Mgal/d)-- - - - Percentage of total ground water-Percentage of total irrigation - - 70 • 9 12 148 140 18 JOO 51 33 4 85 490 64 6 17 39 • 5 30 Hills area has dissolved-solids concentrations less than 25 milligrams per liter (mg/L) and hardness less than JO mg/Las calcium carbonate; the pH commonly is below 6, making it corrosive. Sands that form the Outer Banks are the only source of freshwater along much of the northeastern coast. The freshwater in these sands often has a dissolved-solids concentration of 500 rng/L and hardness of about 200 mg/L as calcium carbonate. On the mainland north of Pamlico Sound, the surficial aquifer ranges from 50 to 200 ft thick and may yield as much as I million gallons per day (Mgal/d) to single wells or small well fields. Here, water from the aquifer usually has dissolved-solids concentrations of less than 200 mg/L and hardness of less than I 00 mg/L as calcium carbon-ate; the pH, however, may be as low as 5, which renders the :; ,! ! I .I ,, ; .i. I( r i I ,\ ; ' I I I I I I I I I I I I I I I I I 330 National Water Summary__.:Ground-Water Resources Table 2. Aquifer and well characteristics in North Carolina [Ft = feet; gal/min = gallons per minute; mg/L = milligrams per liter. Sources: Reports of the U.S. Geological Survey and the North Carolina Department of Natural Resources and Community Development] .. Well characteristics Aquifer name and description Depth (ft) Yield (gal/min) Remarks Common May Common May ... :• range exceed range exceed Surficial aquifer: Sand, silt, clay, and gravel. Generally unconfined or partially confined. Yorktown aquifer: Sands and clay. Partially confined or confined. Castle Hayne aquifer: Limestone, sandy limestone, and sand. Generally confined. Cretaceous aquifer: Sand, clayey sand, and clay. Confined. Crystalline rock aquifer: Crystalline igneous, mCrlasedimentary and metavolcanic rock. Semiconfined to confined. 40-65 175 50-150 190 70-200 400 100-600 800 75 -200 300 water corrosive. The aquifer generally is unconfined to par- tially confined throughout most of the Coastal Plain, but where it is more than 50 ft thick, water usually is confined in the deeper parts due to differences in lithology. YORKTOWN AQUIFER The Yorktown aquifer is present at shallow depths in the northern Coastal Plain. A few high-producing wells tap the Yorktown. Elizabeth City in Pasquotank County draws 1.3 Mgal/d from a well field that taps the aquifer. Water in the Yorktown aquifer generally has dissolved-solids concentra- tions of less than 500 mg/L and hardness of less than 300 mg/Las calcium carbonate. CASTLE HAYNE AQUIFER The Castle Hayne aquifer is the most productive aquifer in North Carolina. Wells that yield more than 1,000 gallons per minute (gal/min) can be readily developed in this aquifer and yields may exceed 2,000 gal/min. The Castle Hayne is the major source of freshwater in the southeastern coastal area where nearly all other aquifers contain some saltwater. Water from the Castle Hayne aquifer usually has a hardness ranging from 80 to 300 mg/L as calcium carbonate (Wilder and others, 25 -200 IS -90 200-500 200-400 5-35 500 Important aquifer in Sand Hills, northeast North Carolina, and Outer Banks. Water only slightly mineralized, except at depth in coastal areas where it is salty. Iron problems common. Equivalent to Columbia aquifer in Virginia. 500 Includes Yorktown Formation and minor sands in Pungo River Formation. Important aquifer in northern Coastal Plain. Water is salty in coastal areas. Iron problems common. Equivalent to Yorktown-Eastover aquifer in Virginia. 2,000 Includes Belgrade and River Bend Formations, Castle Hayne Limestone and Beaufort Formation. Castle Hayne Limestone is major aquifer in eastern Coastal Plain. Iron and hydrogen 1,400 200 sulfide are problems near aquifer's western limit. Water is salty at depth near coast. _,/ Includes Peedee, Black Creek, and Cape Fear Formations. Most widely used aquifer in Coastal Plain. Water has low mineral content. Iron problems common. Water is salty at depth in eastern Coastal Plain. Equivalent to Potomac aquifer in Virginia and Black Creek and Middendorf aquifers in South Carolina. Large well yields dependent on interception of fractures; sustained yields dependent on thickness of saturated regolith overlying fractured- rock aquifer. Dissolved Solids average about 170 mg/L. Water slightly acidic and may be corrosive. Locally high in iron and silica. 1978) and requires treatment for some uses. It commonly contains concentrations of silica higher than 50 mg/L. The aquifer generally is confined, except near its western limit where it is unconfined or partially confined. CRETACEOUS AQUIFER .... ~ ;;i . t:· _,,.: -;~; ,\ri! --=~·, /J.;.~~ . ~-· ·-· ,-. i~~ FJ:-:. ·-• • ·,y,. .,:;{ :;:g -•~5.:£---•'-f'-•·-"'ffl..:: •-Ja,.;;" .__,,., . The Cretaceous aquifer is the principal aquifer in much of the central and southern Coastal Plain. The aquifer has only moderate hydraulic conductivity but is very thick. For this reason, a number of well fields in the Cretaceous aquifer are ·-= able to produce more than 1 Mgal/d. Water from the Creta-. _ . · ceous aquifer typically is soft with hardness commonly less . ; than 20 mg/L as calcium carbonate. The water occasionally ~~-:. t contains concentrations of fluoride higher than 1.5 mg/L, the."-?'~~ maximum limit for public supplies in this area. The aquifer is :t,,it'" confined throughout its areal extent. . ..:~z.:.,. .. --~ '-\(({'i CRYSTALLINE ROCK AQUIFER -·i'f The crystalline rock aquifers of the Piedmont and B!ue 1F~--· Ridge provinces consist generally of fractured cryst:i!!,ine igneous and metamorphic rock that has low porosity and, therefore, little storage capacity. Well yields are sustained by water stored in the saturated regolith that overlies the f~a~.- ' EXPLANATION □ Surficial aquifer 1~.11 Su rficial aquifer and .~· Yorktown aquifer Yorktown aquifer Castle Hayne aquifer Castle Hayne aquifer and Cretaceous aquifer Cretaceous aquifer Crystalline rock aquifer Not a principal aquifer A-A' Trace of cross section A Sea level -1000' -2000' C National Water Summary-North Carolina 0 50 100 MILES A' 0 20 40 MILES Figure 1. Principal aquifers of North Carolina. A, Geographic distribution. B, Physiographic diagram and divisions. C, General- ized cross section (A-A'}, Coastal Plain. (See table 2 for more detailed description of aquifers. Sources: A, C, compiled by R. W. Coble from U.S. Geological Survey and North Carolina Department of Natural Resources and Community Development files. 8, Fenneman, 1938; Raisz, 1954.} · 331 I· I I I I I I I I I I I I I I I I I I 332 National Water Summary-Ground-Water Resources tured bedrock. Success in constructing high-yield wells in this terrane depends on interception of water-bearing fracture systems that are overlain by saturated regolith. The chance of intercepting interconnected fractures is greatest in valleys and draws and least on ridges and hilltops. The average yield of wells in the crystalline rock is low-about IO to 25 gal/min; however, yields of 200 gal/min or more are common. Water from the crystalline rock has a dissolved-solids concentration that is commonly about 170 mg/L and rarely exceeds 250 mg/L. Hardness generally is less than 100 mg/L as calcium carbonate. Because of the low buffering capacity of the water, corrosion can be a problem where the dissolved-solids concen- tration is less than 100 mg/L, even though pH values range from 6.3 to 6.7. OTHER AQUIFERS Triassic basins within the crystalline rock terrane of the Piedmont are areas from which the principal aciuifers are absent (fig. I); these basins consist of downfaulted blocks of crystalline rock. The basins are filled with clay, silt, fine- grained sandstone, and conglomerate, into which, in some places, basalt dikes have intruded. In this terrane, chances of constructing wells that yield more than a few gallons per minute are slight. GROUND-WATER WITHDRAWALS AND WATER-LEVEL TRENDS Major areas of ground-water withdrawals and water levels for selected observation wells near pumping centers are shown in figure 2. Generally, water levels decline in response to increases in pumping and recover when pumping is reduced. The hydrographs in figure 2 are representative of response of water levels to pumping in the Coastal Plairi. Water-level declines are not widespread in the surficial aquifer. Pumping I Mgal/d from a battery of shallow wells near Elizabeth City (near location I, fig. 2) _ resulted in no measurable decline in water level in an observation well only 0.5 mile (mi) from the well field. Only minor withdrawals are made from the Yorktown aquifer, which is readily recharged; thus, major areal water- level declines have not occurred in this aquifer. In the Belhav- en area, withdrawals of 1.2 Mgal/d have resulted in less than 10 ft of decline in 16 years as shown by the hydrograph (location 5, fig. 2). The largest ground-water withdrawals in North Carolina are from the Castle Hayne aquifer to dewater one mine and three quarries. About 65 Mgal/d are withdrawn from the confined Castle Hayne aquifer to reduce the artesian pressure, thereby facilitating dewatering of the overlying phosphate ore beds. Water levels in the Castle Hayne have declined 5 ft or more over an area of 1,300 square miles in response to this pumping (North Carolina Groundwater Section, 1974). The hydrograph for the Castle Hayne observation well, which is adjacent to the mining area (location 6, fig. 2), shows the rapid decline in water level when pumping began in 1965; stabilization of the water level was achieved in 1966 when the amount of induced leakage into the aquifer and a reduction in the amount of natural discharge from the aquifer compensat- ed for the amounts of withdrawal. Changes in water level since the late 1960's are the result of fluctuating pumping rates and movement of the center of pumping as different parts of the· ore body are mined. Other withdrawals from the Castle Hayne aquifer range from 11 to 18 Mgal/d at three quarries (locations 8, 11, I 6, fig. 2). Because the Castle Hayne general- ly is unconfined in the area of the quarries, the geographic extent of the cones of depression is limited. Widespread withdrawals from the Cretaceous aquifer · have resulted in continuing declines in water levels in this aquifer throughout much of the Coastal Plain. The Creta- ceous aquifer observation well (location 7, fig. 2) reveals that, after a well field was established near the observation well in 1968, water levels have declined more than 80 ft. Periods of water-level recovery and apparent stability are the result of short periods of decreased withdrawal rates. Water levels in the Cretaceous aquifer in the northern Coastal Plain have declined over an area of several thousand square miles in North Carolina because of withdrawals of 35 Mgal/d or more near Franklin, Va., 10 mi north of the State line. Declines near the line (location 26, fig. 2) have been as much as 45 ft since 1966 and are estimated to be as much as 100 ft since the early 1940's when extensive withdrawals began. Water-level declines because of withdrawals from the crystalline rock aquifer are not widespread. Water pumped from the aquifer is supplied from the saturated portion of the overlying regolith. Recent research shows that withdrawals from the crystalline rock aquifer are reflected in local cones of depression in the overlying regolith (Daniel and Sharpless, 1983). GROUND-WATER MANAGEMENT --~:;;.11'· -~,-,,~, ·:fr.:~ : ?. ;·_,,l •~fl -" :fml The North Carolina Department of Natural Resources :;~~,~ and Community Development (NRCD) implements most of .. ~-J:~ the regulatory and planning procedures related to grouncf--< :_t.4 water resources in the State. The Division of Environmental · ~"?•~· Management (DEM) within NRCD, has the major responsibil-\.J~ffit. l ity for ground-water management and regulatory programs. -'·, •-'.,~.:ii.ti The Environmental Management Commission has authority , ..... ,1 over the pi;rmitting process and has made the Groundwater -.,.A~~{ Section of DEM directly responsible for issuing permits for -~i1it; well construction and ground-water withdrawals. The Com-·~·:~ mission may designate an area as a Capacity-Use Area .. ;.;~:?~ · whenever the renewal and replenishment of the ground-water ~~,~ supplies are believed to be threatened. To date, the Commis-• ;::'l.~- sion has established only one such area in east-central North ·--~rf! . Carolina. However, additional areas are being considered for --~ Capacity-Use Area designation. ·;'.~~'!~ A permit must be obtained from the Groundwater Sec--;~~..:i~ tion of DEM for (I) the construction of public-supply, indus-... ::½;~i •. trial, and irrigation wells, (2) wells with a designed capacity of -";;) 1 100,000 gallons per day (gal/d) or greater, (3) wells to be used _.;~~I, for injection, recharge, or disposal purposes, and (4) a well, · 'i:.,~t, other than a domestic well, located in a designated Capacity-, ..:.1~ Use Area (North Carolina Well Construction Act of· 1967, -~·i•~ Article 7-87-88). Injection wells for waste-disposal purposes -1~:.tf' currently are prohibited by State statute. All well drillers must ·. ".•t~f register annually with NRCD and are required to report all .,· well completion and abandonments. ~:4· In addition to a water-use permit in Capacity-Use Areas ---~~ for users withdrawing more than 100,000 gal/d, NRCD also ::;:l':,,, may require these users to adhere to established maximum . ;,;r~~ withdrawal rates; the agency also can establish the minimum -...::::2'. ~ water levels resulting from pumping in certain areas. ~itr The NRCD pivision of Water Resources (DWR) collects· '4M data on the use of ground water statewide through its water• -,;,_·r.,l use data program. The DWR includes ground water in special • ......,_~ regional or river basin water-resources studies with primary .~}fJr, emphasis on the availability of ground water to meet w~ter-· -~,.~~-~ l.; supply needs for municipal and industrial use and for agncul-; -.'-/:if'lt..V.S tural irrigation. The DWR also provides technical assistanc~ ,:,~~l~}t1:f to local goverment water utilities in considering ground water . '•\~~miiiti.,,."' . . I , ... ·11!Jli/<_.~ , as a. source of supply for public-water systems. Techmca ; •. :J[@:&',~-t · information on ground water is also available through the · · · .•t~~ Iii '► ,\ ' • ::;!:· ,; '· To: File /~ From: G.Doug Rumford~ Date: 6/12/95 Subject: Weyerhauser Co.-Plymouth Plymouth, Martin County, NC NCO 991 278 540 REF. 25 Memorandum Telephone Conversation with Mr. Harold Mccarson On this day, I spoke with Mr. Harold Mccarson (919-793-9466), Business Development Manager with Hydrologic, Inc., the company that administers the Plymouth water system. Mr. Mccarson told me that the city system is supplied by 4 groundwater wells; 3 of the wells are approximately 185 ft deep and 1 well is approx. 115 ft deep. The Plymouth water system supplies drinking water to about 4119 people within the city limits. Washington County purchases water for distribution to residents outside the city limits. According to Mr. Mccarson, the water system is sampled on a yearly basis for VOC'S, SVOC'S, and inorganics and has not shown any indications of contamination. Mr. Lee Smith, County Manager of Washington County was also contacted. He confirmed that the county buys water from the city for distribution outside of the cityJjmits. The county provides water to 1850 customers. __ , ?W·NW t @liLrm IIWW ' __ ,.. ·~· .. ~ ~-- I I I I g n u I I I I I I I I I I I I MEMO TO: FROM: Superfund Section Staff Jeanette Stanley Environmental Chemist NC Superfund Section DATE: August 15, 1996 REF. 26 SUBJECT: Update on Status of Wellhead Protection Programs in N.C. I spoke with Mr. Randy Prillaman, Hydrogeologist, NC DEM (919) 715-6187. He said that the Wellhead Protection Area implementation plan written by him and submitted to US EPA in late Dece~ber I 994 has been approved. This plan calls for protection of a whole ·area based on a calculation using recharge rate and pumping rate as variables. North Carolina now has primacy in approval of wellhead protection areas. None have yet been implemented. Several requests for approval have been received but no areas have yet been approved. Mr. Prillaman said that he could not project a date when a plan would be approved. ,. I I 0 I I I I I I I I I I I REF. 27 Memorandum To: File From: G.Doug Rumford Date: 10/11/96 Subject: Georgia-Pacific Corp. Hardwood Sawmill Plymouth, Washington County, NC NCD 000 813 592 Groundwater Population within 4-mile radius The population of groundwater users within a 4-mile radius of the site was estimated by utilizing a topographic map house count and identifying the extent of the town water distribution system. The extent of the Plymouth City and Washington County water system was determined by referring to Figure 3 of the Greenhorne and O'Mara Phase II SSI Report for Georgia-Pacific Hardwood Sawmill. The water lines were then superimposed on the Georgia-Pacific site topo map (Fig. 1) and the residences without access to the system were counted as private well users. This was accomplished by a topographic map house count combined with a windshield survey within the 1 /2-mile distance ring. The nearest groundwater residence is located approx. 1.3 mile east. According to the 1990 census, there are 2.72 persons persons per household in Washington County. The number of people served by the city water system( 4119 city; 1850 county) was added to the groundwater user population within the1-2 mile distance ring as this is where the wells are located. No community wells other than the Plymouth city wells were identified by the NC Public Water Supply System database. Distance Ring G.W. Residences Groundwater Pop 0-1/4 mi. 0 0 1/4 -1/2 0 0 1/2 -I 0 0 I -2 7 5989 2-3 145 395 3-4 194 528 Total 346 6912 I Attachment. I I I I --I!!!!! I!!!!!!! liiiiiil liiii iiiil iiilil --l!!!!!!!!I l!!!!!!I l!!!!!!'l REF. 28 . f'ly,,.o,v-/1--. ?r-lfDt. -"1-7 / 'i ·7~;J.,."f;:) ;;;_ 7 . 1,,/ r-> / hL ?I rtWt .I/-71 3 -'i 1../ b t., Cr?-/( /( f'I?"' ,,v,t,,€c/ ff~J:.,lf r',-v/ . HAROLD F. McC11, ,~(Jei, vf1. .. , . ("'/tJ/L/4-. BUSINESS D[VEL0/lfv1[:,Jl Mr\r~AG.ER HYDRO[OGIC~ INC P . .:· 3GX 13029 ;,s:-iEViLl.E. r~c 23814-002S : ,:1,:_::1cE: ?o.i-25,:_5,G9 TOl.~ FREE: (l00-23~-8&&~1 ::z"·LYr.':/l.;; STHEd f\SHEIJ!LLE, :\:C 2.e80i i'.;iX:)04,-252-9711 ! iOidE'. 704-667 :S8GG RECEIVED MAY l l 7995 SUPERFUND SECTION ......... ,'./•, . ~s.'~;®W~[f®liOlliID@UOU TI 9 ~UO@®[f~®~Glfr@@l II .. ··_· ;!c._ ·."!: .. 11 LABORATORY ID#, 37715 WATER SYSTEM ID#, 04-94-010 NAME OF SYSTEM, TOI-/N OF PLYMOUTH ·sYSTEH TYPE, (E) (E=ENTRY POINT; COUNTY: WASHINGTON S=SPECIAL; W=SOURC~) TIME1' 08: 10 AM·<;•/ ... , ,.·, COLLECTED ON: 01/10/95 LOCATION WHERE COLLECTED: LOCATION/SOURCE CODE: 001 809 WASHINGTON STREET (WATER PLANT) COLLECTED BY.r WILLIE C. DAVIS HAIL RESULTS TO, 'fYPE Ol,' SYSTEM ( X ) .. ..CO~H-IUNITY .( ·) NTNC RECEIVE.D MAY 111995 SUPERFUND SECTION au II TOWN OF PLYMOUTH P.O. BOX 806 ( ) NON-COMMUNITY ( ) PRIVA'J;E PLYMOUTH, NC 27962 II WATER SOURCE -TELEPHONE·; (919) 793.:9101 ... -· -. -·-·· -.-:· .· . -?l ~~~~~~E ,r·--c~~~~ .. ---·--·-.... ·---~~;~----· --·····-~W II· .. ~~~P:~:::HENT --..•.. .::.. .• _. CODE NAME CODE RESULTS LIMITS II ( ) NONE ii ~;;;·-~;~~~;~-~;~~-----------~;;---:;~;~;----;~;;;--11 ix! ~~~:i~:~~g ,...,~,-1010 BARIUM, mg/1 125 <0.100 2.000 II ( ) FILTERED ' '·· ..• 1015 CADMIUM, mg/1 125 <0,001 0.005 II ( ) ALUM 1020 CHROMIUM, mg/1 125 <0.005 0.100 II ( ) LIME ~.. 1024 CYANIDE, mg/1 . 148 <0.005 0.100 II ( ) SODA ASH I.::· __ 1025,,.FLUORIDE, mg/1 107 0.74 4.000 II ( ) CAUSTIC 1028 IRON, mg/1 101 0.013 0.300 II ( ) WATER SOFTENER :. · 1032 MANGANESE, mg/1 101 <0.010 0.050 II ( ) POTASSIUM PERMAN. ,,,_· -.•• 1035 MERCURY, mg/1 103 <0.0002 0.002 II ( ) P04, IRON CONTROL • 1036 NICKEL, mg/1 101 <0,010 0.100 II { ) P04, HANG. CONTROL ~ -1045 SELENIUM, mg/1 125 <0.010 0.050 II ( ) P04, CORR. CONTROL c.=.~ 1052 SODIUM, mg/1 101 298.0 NIA l,L'=={=)=O=TH=E=R=•;;;;~---,_ · 1055 SULl'ATE, mg/1 137 37 N/A Ir Iii! · 1074 ANTIMONY, mg/1 125 <0.0012 0.006 II ~ -1075 BERYLLIUM, mg/1 125 <0.0001 0;004 II if',:;,,•.. 1085 THALLIUM, mg/1 125 <0.001 0.002 II l==--1925 pH, Units 135 7. 7 G 6. 5 II II I LABORATORY NOTE A result preceded by the 'less than' symbol must be less than the standard or QC used which must be one-fifth (1/5) of the allowable limit. ,.-( ) SAMPLE UNSATISFAC'rDRY -( ) RESAHPLE REQUESTED :: ~te· Analyses Begun, . 01/10/95 Time Analyses Begun, 2,00 PH Time Analyses Completed, 5:00 PH te Analyses Completed: 01/24/95 Certified By, DB tnments, i·· I-;0039 ~(-. . , ...:::!!;·,. - Laboratory Analyses -Environmental Consultants •• ••-•--•• "• • • •-•• •• • •• •• • ••·. • • • _,,..:..:• ..... -~•••• ••••• •• •• ••'·.,-.•-•,...,__,-• A-~•:•~--• •n ·••••~ _ ...... ••--•-• ••·•-••-•• ~••••· •~•• ~• • ·''-"· .,, .. ..,~-· - -,·:ooworr®uouilil@UOfr TI 9 ~uo©®D'~®D'®fr@r~J -·-- , P.O •. BOX 7085, 114 OAKMONT DRIVE · . PHONE (919) 756-6208 r .. · ~1;1:!iYIJ,,..l-1:, .N,Q,. 2~35:70~? .. .... . . ..... ··-.: ; .. · ..... , . , . . . ... · ............. , •• ~ •.• ,.,: .• ~, : .... "'·''··~·-• ... .fl\?'.<. (!lWl ?~§:Q§~~- '. ~ -. -~·.-. 11>: .I.J\BORATORY ID#, 37715 NITRJ>.TE_/NITRITE. :c. ·_:::_WATER-SYSTEH ·ID#·c 04-94-010 .. COUNTY: WASHINGTON. II· '" NAME OF SYSTEM, TOWN OF PLYMOUTH r · .,. SAMPLE TYPE, ( E ) ( Em ENTRY; SaSPECIAL) . _~COLLECTED ON DATE, 01/17/95 (MM/DD/YY) TIME, 07, 10 AH(Ht!,MM AM OR PM) Ii · LOCATION WHERE COLLECTED: ·~ ;, ~CATION/SOURCE CODE, 001 COLLECTED. BY1 WILLIE C. DAVIS ' , .. MAIL RESULTS TO: TOWN OF PLYMOUTH P.O. BOX 806 PLYMOUTH, NC 27962 TYPE OF SYSTEM ( X) COMMUNITY ( ) N'fNC ( ) NON-COIIMIJNI'rY (. ) PRIVATE p--TELEPHONE (919) 793-9101 ( X) GROUND ( ) SURFACE ~------L-... l.Y..I.J~~~!L_. _ __,... ) SAMPLE UNSATISFACTORY TYPE TREATMENT, ( ) NONE ( X) CHLORINATED ( ) FLUORIDATED ( ) FILTERED ( ) ALUM ( ) LIME ( . ) SODA ASH ( ) CAUSTIC ( ) WATER SOFTENER ( ) POTASSIUM PERMAN. ( ) P04, IRON CONTROL ( ) P04, HANG. CONTROL ( ) P04, CORR.CONTROL ( ) OTHER ___ _ j c:z::1:z::.:;11a::;.=ca1:1.::i::1.mmcmsi1:11:c:>m••==-=a=:ic~. ·', .-•••• , • _._ .. , .:.-:·:-. • • ;_ ••.· :,.:.~-·---,. •• : >-. .: • ,~: '·":" -· ) RESAMPLE REQUESTED 'l'IHE ANALYSIS BEGUN, 02100 PM TIME ANALYSIS COMPLETED,05,00 PH CERTH'IED BY, DB Laboratory Analyses -:-. Environmen_tal Consult9f/(S:F ,, ,,'.:'. ·.: : i , . , . • . ... .• .•••.. . , ....•.•.. ··-··-···· • ... ,. -----· ·---~---·-·--, _______ .,.• .. , ........... ·.~·· ... ., •.••. ,, .,u:. •• :.:i....:.--.; __ f,.L ... --_...,\ ___ , ---···-·--_ "'-, .... , : . I:,;·· . '·( i,.<,:•.~"- . -·'LABORATORY ID#: 37715 I~ WATER SYSTEM ID#, 04-94-010 NAME OF SYSTEM, TOWN OF PLYMOUTH . - COUNTY, WASHINGTON RECEIVED MAY 111995 SYSTEM TYPE, ( E) (EaEntry Point; S Special) i . ·coLLECTED ON, 10/19/93 (HH/DD/YY) TIME: 8:00 AH(HH:HH AM or PM .. LOCATION WHERE COLLECTED 1 . 809. WASHINGTON STREET :-: .. .WATER PLANT. ·-. . .. LOCATION/SOURCE CODE: 001 COLLECTED BY, JOHN W. CARROLL SUPERFUND SECTION I :, HAIL RESULTS TO, I ,. 1·r·:. TOWN OF PLYMOUTH P.O. BOX 806 PLYMOUTH, NC 27962 TYPE OF SYSTEM ( X) COHHUNITY ( ) NTNC ( ) NON-COMMUNITY ( ) PRIVATE WATER SOURCE ( X) GROUND · · TELEPHONE, (919) 793-9466 ( ) SURFACE ,_: ____________________________________________________ ~---~-:~~=~~~------------------------ . , • NOT I CONTAH HETH. DETECT. DETEC. QUANT. ALLOW. REGULATED(R) CODE CONTAMINATE CODE LIMITS (X) RESUL'l'S LIMITS UNREGULATED(U; ---------------------------------------------------------.. :: 2005 I 2010 2015 , 2020 I ;:~;··• . '2031 f;1 2032 1--2033 : 2034 ,. 2035 I.., 2036 . ;-2037 • 2040 12041 2042 -·-2043 12044 . 2045 .. ,. Endrin, mg/1 Lindane, rng/1 Methoxychlor, rng/1 Toxaphene, rng/1 Carbary!, mg/1 Hethornyl, mg/1 Dalapon, mg/1 Diquat, mg/1 Endothall, rng/1 Glyphosate, rng/1 Di-2(ethylhexyl)adipate, mg/1 Oxarnyl (vydate), mg/1 Simazine, rng/1 Piclorarn, rng/1 Dinoseb, mg/1 Hexachlorocyclopentadiene, mg/1 Aldicarb Sulfoxide, mg/1 Aldicarb Sulfone, mg/1 Metolachlor, mg/1 . 204 204 204 204 . ... 235 .. 235 203 242 241 240 206 235 207 203 203 204 235 235 207 0.00001 X 0.002 R 0.00002 X 0.0002 R 0.0001 X 0.04 R 0.001 X 0.003 R 0.00073 ... X .. · ........ ____ . N/A :-.J·•• ·.u.,. 0.00016 X N/A u 0.001 X 0.2 u 0.0004 X 0.02 u 0.009 X 0.1 u 0.006 X 0.7 u 0.0006 X 0.2 u 0.002 X 0.07 R 0.00007 X 0.004 u 0.0001 X 0.5 u 0.0002 X 0.007 u 0.0001 X 0.05 u 0.0005 X 0.004 R 0.0008 X 0.003 R 0.00036 X N/A u IJ~~~~~;f,~J~ey;~iJ;t@~i.;L~4;{~£~.:i:'::~:,:jJ~,;~;si;~~~~~;;;;;;~;,;;tf~~~i;j;.fa~~~tP1£4,~J;Jk~2;~i ;~,,~;'.~;-,;_,;;:;.;_:~,.i-L~",'• ·_ .. ·:.·:,.;1:;~L P.O. BOX 7085, 114 OAKMONT DRIVE . .. . ,,_, _ _ . ":' • i-,, _._ . PHONE (919) 756-6208 . IR!f f SY!l.l,E:,. !':!.-.C,.£?83§-?ll~!? ., ..... ---·.-;, ..•. ,.~:~.x;..c;~'.,;,'--'i-:c::!~L""~"~"" "'"'-'-'·'·'-'''""'~';""'°'····--, •·' .• , .. "· fM (~1 ~) .. 7§§-:9.§~ •. .. PESTICIDES AND SYN'rHETIC ORGANIC CHEMICALS (continued) I LABORATORY ID#: 37715 1· COLLECTION DATE, I CONTAM CODE 10/ 19/93 CONTAMINATE I ;~~~ 2047 12050 2051 2063 2065 · i. 2066 2067 2070 2076 I·. 2077 2105 2110 i 2274 2298 2306 i 2326 2356 2383 2440 i 2595 '2931 · 2946 12959 · . ' ---~ ---. ·-. ' .•. Carbofuran, mg/1 Aldicarb, mg/1 Atrazine, mg/1 Alachlor, mg/1 2,3,7,8-TCDD(Dioxin), mg/1 Heptachlor, mg/1 3-Hydroxycarbofuran, mg/1 Heptachlor Epoxide, mg/1 Dieldrin, mg/1 Butachlor, mg/1 Propachlor, mg/1 2,4-D, mg/1 2,4,5-TP (Silvex), mg/1 Hexachlorobenzene, mg/1 Di-2(ethyhexyl)phathalate, mg/1 Benzo(a)pyrene, mg/1 Pentachlorophenol, mg/1 Aldrin, mg/1 PCB's, mg/1 Dicamba, mg/1 Hetribuzin, mg/1 DBCP, mg/1 Ethylene Dibromide (EDB), mg/1 Chlordane, mg/1 SAMPLE UNSATISFACTORY ('nate Analyses Begun: . 10/19/93 l--1:_~te Analyses Completed, 01/17/94 • Laboratory Log# 8115-101993-001 _Comments, Contaminant codes 2032, 2105, & · . When analyzed, contaminant code 1-:-' 1· WATER SYSTEM ID#, 04-94-010 LOCATION/SOURCE CODE, 001 NOT HETH. DETECT. DETEC. QUANT. ALLOW. REGULATED ( R) CODE LIMITS (X) RESULTS LIMITS UNREGULATED(! ------------------------ 235 0.0008 X 0.04 235 0,0005 X 0.003 207 0.0001 X 0.003 204 0.00002 X 0.002 250 5.00E-09 X 3.0E-08 204 0.00004 X 0.0004 235 0.00063 X N/A 204 0.00004 X 0.0002 204 0.000008 X N/A 207 0.0037 X N/A 207 0.0027 X NIA 203 0.0001 X 0.07 203 0.0002 X 0.05 204 0.0001 X 0.001 206 0.0006 X 0.006 243 0.00002 X 0.0002 203 0.00004 X 0.001 204 0.00002 X N/A 204 0.0001 X 0.001 203 0.00030 X N/A 207 0.00039 X N/A 219 0.00002 X 0.0002 219 0.00001 X 0.00005 204 0.0002 X 0.002 RESAMPLE REQUESTED Time Analyses Begun: 3,00 PH Time Analyses Completed, 4:00 PH Certified By, DB 2033 by laboratory #18700. 2063 by laboratory #37747. R R R R u R u R u u u R R u u u R u R u u R R R I . . . · Laboratory Analyses . ..,.. Environmental Consultants/.i.:"'·>i•. --·· ·. / 1039 ..... ··•·-· .... · ... " .. ··•····· -.... c._c .• , ... r. ..• -~---........ -C ..• ..o.s----'-'--" "'"''-"--~-'-'-" '-~"'"""'-"'-"""'-'--'"''"'-'-'=•2;,e~.::Cc&,;,~.;.,,_.;,"'·•'··•c ...... c I w·z ITWdYP"''W'!C-ci'::e:::ne:rrnwmtli:ifT~Y!f?lr3/::~Z::1!'iffli:e\'N:?f1 ~-:1 ~ foo-~□U'®mJOiJil@OO,fr _ TI~ ~oo@®U'OJ®U'GJfr@@l ,.·' . . . , ... LABORATORY ID#, 37715. WATER SYSTEM ID#, 04-94-010 COUNTY, WASHINGTON . NAME OF SYSTEM: TOWN OF PLYMOUTH _ I--SYSTEM TYPE, ( E ) (EcEntry Point; SmS_pecial; WmSource) . -COLLECTED ON: 06/14/94 (MM/DD/YY) TIME: 08:00 AH(HH,H!1 AM or PM) -LOCATION WHERE COLLECTED: 809 WASHING1'0N ST -WATER PLANT i: WCATION/SOURCE CODE: 001 COLLECTED BY, JOHN CANSIU. TYPE OF SYSTEM I MAIL RESULTS 'fO, ( X ) COMMUNITY ( ) NTNC 'I'Olftl OF PLYMOUTH ( ) NON-COMMUN!l'Y I 806 BOX ( ) PRIVA1'E PLYMOUTH, N.C. 27962 1'YPE 'rREA'rHEN'r ( ) NON-CHLORINATED I 1'ET,EP~O~:__( 9_1_9_), '.:3~=•-~--66--■-•---~---~---~--c __ .... __ (-~~~-=~~=N~=~?. __ c-~--~ --,~c O ___ -" CON'rAH MJ::THOD DETECTION DETECTED QUANTIFIED ALLOW. CODE CON'rAMINATE CODE LIMITS (X) RESUL'!'S LIMITS -------------------------------------------------------------p-Isopropyltoluene, mg/1 217 0.0005 X N/A Chloromethane; mg/1 217 0.0005 X N/A DCDfluormethane, mg/1 217 0.0005 X NII\ Bromomethane, mg/1 217 0.0005 X · N/A Chloroethane, mg/1 · 217 0.0005 X N/A ' . Fl uorotnchloromethane, ir,g / l 217 0.0005 X N/A Hexachlorobutadiene, mg/1 217 0,0005 X N/A Naphthalene, mg/1 217 0.0005 X N/A 1,2,4-TChlorobenzene, mg/1 217 0.0005 X 0.07 c-1,2-DChloroethylene, mg/1 217 0.0005 X 0.07 Dibromomethane, mg/1 217 0.0005 X N/A 1,1-Dichloropropene, mg/1 217 0.0005 X N/A 1,3-Dichloropropane, mg/1 217 0.0005 X N/A 1,3-Dichloropropene, mg/1 217 0.0005 X NIA 1, 2, 3-TChloropropane_, mg/1 217 0.0005 X N/A 2,2-Dichloropropane, mg/1 217 0.0005 X NIA 1,2,4-THethylbenzene, mg/1 217 0.0005 X N/A 1,2,3-TChlorobenzene, mg/1 217 0.0005 X N/A n-Butylbcnzene, mg/1 217 0.0005 X N/A 1,3,5-THBenzene, mg/1 217 0.0005 X N/A tert-Butylbenzene, mg/1 217 0.0005 X N/A sec-Butylbenzene, mg/1 217 0.0005 X N/A Bromochloromethane, rug/1 217 0.0005 X N/A Chlorofonn, mgll 217 0.0005 X A Bromof on1,, mg/1 217 0.0005 0.0160_ N/A REGULATED (R,U) u u u u u u u u R R u u u u u u u u u u u u u u u VOLATILE ORGANIC CHEMICALS(continued) I . 2943 BDChloromethar,e, 111,;tl 2944 CDBromomethane, mg/ 1 · 2955 Xylenes (Total), mg/1 •~0_ 2964 Dichloromethane, mg/ 1 ' . -2965 o.:.Chlorotoluene, mg/1 . 2966 p-Chlorotoluene, mg/1 ·· • ·. · 2967 . m-Dichlorobenzene, mg/1 ' ';..;.. 2968 o-Dichlorobenzene, mg/1 -2%·99--np-01chlorobe11zene, 111911· . ,. 2976 Vinyl Chloride, mg/1 ' . · ·,_·--2977 1, 1-DCEthylene, mg/1 .. 2978 1,1-DCEthane, mg/1 fc 2979 t-1,2-DCEthylene, mg/1 .,-,.,;.,;-;,:-2980 1, 2-Dichloroethane, mg/ 1 l :'.~2981 1,1,1-TCEthane, mg/1 .',; ·2982. Carbon Tetrachloride, mg/1 -~ · .~. · 2983 1, 2-Dichloropropane, mg/1 ' ' · ·::: •. ·2984 t' Trichloroethylene, mg/1 ,',. 2985 1, 1,2-TCEthane, mg/1 .,,:.c,c 2986 .1, 1, 1, 2-TCEtharie, mg/ 1 •:,-.ci';/ 2987 TChloroer.hylene, mg/1 l-:···2988 · 1,1,2,2-TCEthane, mg/1 :7'.: 2989 Chlorobenzene,mg/1 •.,."'.''. 2990 · Benzene, mg/ 1 I. · 2991 Toluene, mg/1 :.2 2992 Ethylbenzene, mg/1 ...,.::.;;2993 Bromobenzene, mg/1 ' ,.·: 2994 Isopropylbenzene, mg/1 .,,...2996 Styrene, mg/1 c-·2998 n~Propylbenzene, mgll If·( J SAMPLE UNSATISFACTORY I·,= Date Analyses Begun, 06-14-94 ~ Date Analyses Completed, 06-27-94 . Comments, I. ,_~-Laboratory Log # 8115-061494-001 NOT WATER SYSTEM ID#, 04-94-010 LOCATION/SOURCE CODE: 001 METHOD DE'fECTION DETEC'l'ED QUAN'1' rnco ALLOl4. REGULATED CODE LIMITS (X) RESULTS LlHI'fS (R,U) ------ 217 217 217 217 217 217 217 217 21/ 217 217 217 217 217 217 217 217 217 217 217 217 217 217 217 217 217 217 217 217 217 --------------------------0.0005 0.0011 0.0005 0.0048 0.0005 X '. 0.0005 X · 10.0005 X 0.0005 X 0.0005 X 0.0005 X 0.0005 X 0.0005 X 0.0005 X 0.0005 X 0.0005 X 0.0005 X 0.0005 X 0.0005 X 0,0005 X 0.0005 X 0.0005 X 0.0005 X 0.0005 X 0.0005 X 0.0005 X 0,0005 X 0.0005 X 0.0005 X 0.0005 X 0.0005 X 0.0005 X 0.0005· X ... ------ NIA A 10 0.005 NIA N/A NIA 0.6 0.0,j 0.002 0.007 N/A 0.1 0.005 0.2 0.005 0.005 0.005 0.005 Nlh 0.005 N/A 0.1 0.005 1 0,7 NIA NIA 0.1 ., NIA u u R R -U u u R ·H R R u R· R R R R R R u R u R R R R u u R u RESAHPLE REQUESTED 'rime Analyses Begun, Time Analyses completed, Certified By, DB 3,00 PM 4100 PM 10039 ;~,,:c·.c,;c:, ""' '""'.;_.,_"""'"''c""'·"'dc./;-:.~2t~X!;~!ffl~ :;:;:-,£1!!,"!C.'l!.~£!!!/L.fe'!~H!!~!s, ;;';;,, .. ■f Tftzm11St7'=':tt:JllW''T'W::e:fMl·rnw: eu,·r:r:n:r arrnmrerz:n-rec·:n -r -':C'W7"P Subject: Weyerhauser Co.-Plymouth Plymouth, Martin County, NC NCO 991 278 540 Surface Water Pathway Flow Rates REF. 29 Memorandum :rre:w r::r·m•,:i:xrot:t·tez_T":00:::: .. The average annual flow rate for the Roanoke River, 8900 els, was taken directly from the text of USGS Water Supply Paper 2221. The drainage area for Welch Creek was not published in USGS Open-File Report 83-211, therefore, a digital planimeter was used to estimate the creeks' drainage area as 10.4 square miles. Using the mean annual runoff at the site obtained from Water Resources Report 88-4094, the flow rate of Welch Creek was determined; Attachment. ' Drainage Area x runoff / 13.58 = els 10.4 sq.mi. x 15 in/yr/ 13.58 = 11.5 els zr::srrr@1 p p . lriCMlf(f:mr1 wsi:1!'" m .,_ ,,,,, :e: ··a trtil!'rtM:irft'ihlfC: n,u•y » v:rw-r'1etr··we::tte~r:M1itn&df1'♦i"..,,,..lf'I \Nater-Resources Investigations Report 88--1094 MAP OF MEAN ANNUAL RUNOFF FOR THE NORTHEASTERN, SOUTHEASTERN, AND MID-ATLANTIC UNITED STATES, WATER YEARS 1951-80 ) \ \ ) \ \ ·,., .... ·.\:-:· "- M1ssrssrPPr < 0 • \ \ 0 '..::..-:::-. .. ::J~Jl . ·-,-.. ~.-::~~~n <~~J/'.. --~ ~~JI' , ..... ,.,-~ --~-)_, -...· '~ . ~~ ; -. ~ i) 1../' -~/~!·· .. · -,,..;,. r ·---,_ \ Prepared i11 couperatio11 ll'it/z tlze _U.S. l:__nvironmental Protection Agency \..J3f:'.,f-~, , . "'' .. ··:Jt~-. . . .):.:,,,, •~;,)Y.\ I) ,- 1 I I I I I-·: ... .. I .. I: i~ -i i I I sions that the methods that used the area-weighted average of the_ drainage area or. the centroid of the drainage area produced somewhat better correlations-that is, the interecept was closer to zero, the standard errors were small, and the correlation coefficients were larger. These methods have slightly greater power to predict actual runoff Additional statistical investigation found no significant differences in reliability of the runoff estimates among the areas. No significant differences existed in the errors for stations with drainage areas of differing size. USE OF MEAN ANNUAL RUNOFF MAP Mean annual runoff for a site can be estimated from the runoff map by several methods. The simplest method of estimating the runoff is to locate the site on the runoff map and to identify the runoff contour nearest the site. This method, however, is less accurate than other methods. The most accurate method is to draw the drainage basin on the runoff map, and use the runoff contours to divide the basin into bands of differ-ing runoff. The area of each of the bands within the drainage basin is then determined. The areas of the separate bands are then used to compute a weighted average runoff for the basin. For example, if 50 percent of the basin is in an area of 18 in/yr (inches per year) of runoff, 30 percent in an area of 20 in/yr of runoff and 20 percent in an area of 22 in/yr of runoff the mean annual runoff would be calculated as follows: ( 0.5 xl8 + 0.3 X 20 + 0.2 X 22 = 19.4 Runoff estimated from the map is in inches per year, averaged over the entire drainage basin. Multiply this value by the drainage area, in square miles, and divide by 13.58 to convert to mean annual discharge, in cubic feet per second. In the above example, assume the drainage area of the site is 100 mi2. The mean annual discharge, in cubic feet per second, would be: 19.4 xl00/13.58 =143 The runoff map was prepared to allow estimation of mean annual runoff at sites where no streamflow data are available. The map represents mean annual runoff for areas with natural land cover. Caution should be used in applying the map to estimate runoff for areas that are not natural land areas. The runoff map should not be used for areas, such as large urban areas, where the land cover has been altered in ways that would change the amount of runoff. The runoff map is not applicable for lakes or bays, for coastal wetlands affected by tides, for streams controlled by reservoirs large enough to influence the total annual streamflow, or for streams with substantial diversions. Local features could cause the runoff at a particular site to differ substantially from the runoff indicated by the runoff map. The geology of the drainage basin might cause substantial amounts of water to enter or leave the basin as ground water. This could substan-tially increase or decrease the runoff. For example, a stream with a small drainage area that includes a large spring probably would have higher average streamflow than indicated by the runoff map. Table 5.-Descriptive statistics of errors in estimated runoff · at 93 test stations ~ Method Area-weighted Centroid GIS Nearest-inch Nearest contour Area-weighted Centroid GIS Nearest-inch Nearest-contour Mean absolute value 2.0 2.2 2.7 2.8 2.8 9.0 9.8 12.0 12.1 12.2 Mean Error, in inches --0.35 -.71 -1.74 -1.77 -1.79 Percent error --0.54 -.71 -6.42 -6.20 -6.26 Standard error of mean 0.30 .33 .37 .38 .39 1.3 1.4 1.6 1.6 1.6 Standard deviation 2.9 3.1 3.6 3.7 3.8 12.9 13.5 15.9 15.6 15.8 ··-~ ,, -r{;~t.\_ • .. 11 . . . i ·' i ;.. j \, \. :r· rrrcrrrr ·, re, r-·7· r, ·c•·v::::w •w"1c-r··v=:riu1 ·mttc=t>?c'2:Tflt:'5T"'t''IDtaYNh"'VI:....,'IG:'fl2Y:ist"":7"1Y'fM;f;'i1')NS¥'k""'tt!"'ai"!r";'fnt:tw\"f'3!!2':u:ti!'z" l'.·tif }: .. ,: .,: .,_ !-~~efl;'vi lr,•1~t.. · ·•-·· . ~;·.7't.:.:-i,,' . i-:~::··· Hydrology of Major Estuaries I And Sounds of North Carolina 1; By G. L. GIESE, H.B. WILDER, and G. G. PARKER, JR. I i Prepared in cooperation with the North Carolina Department of Natural Resources and Community Development I I I I 1- 1., - i= ·. -' -. -~ ·•. i • i U.S. GEOLOGICAL SURVEY WATER-SUPPLY PAPER 2221 IJ W,---4 + E!!tM?'HPTi:tiW s tt1 n« H?9"eD"Mf?'e?iir' d"'tJDP:TCW,CFU'z'tZftsfli'::i'MC"ll'-:57t:Z:JriC'rm:,(j•·;r-.mm:;:wr:•' t 1 DEPARTMENT OF THE INTERIOR DONALD PAUL HODEL, Secretary U.S. GEOLOGICAL SURVEY Dallas L. Peck, Director UNITED STATES GOVERNMENT PRINTING OFFICE: 1985 For sale by the Distribution Branch, U.S. Geological Survey, 604 South Pickett Street, Alexandria, VA 22304 library of Congress Cataloging in Publication Data Giese, G. L. Hydrology of major estuaries and sounds of North Carolina. · (U.S. G~ologic.:il Survey w.iter-supply pJper; 2221) Bibliography: p. 105 Supt. of Docs. no.: I 19.-13: 2221 1. Estuaries-North Carolina. 2. Sounds Geomorphology- North Carolina. 3. Hydrology-North Carolina. r. \Vi[der, Hugh B. 11. Parker, G. G. Ill. North Carolina. Dept. of Natural Resources and Community Develop- ment. IV. Title. V. Series: Geological Survey water- supply paper ; 2221. GC97.G54 . 1985 551.46'48 85-000158 J ·:e•JHt;ili"R':'8ii':fffl:'tl':;;ws:7i:.,rl?tSX1S'fts".:'-ffl.IW .. l ·--- II 11 I . _, 11- " ._. ·-. ' 1r ... ....... I_ ,_. -, I.:_ -- 1: I I . :i' I '• ,erffiifflf¥~TV'.2li!ff0'1Ntl'3i'tTI::CTh'.S lation. This scatter may he due to several faclor~-the dif- ferences in within-year distribution of discharges, year-to-· year differences in prevailing wind speed and __ direction, and variations in regulation patterns of reservoirs on the Roanoke River which, as previously mentioned, have a direct influence on moderating saltwater intrusion in ·Al- bemarle Sound and. indirectly. into the Chowan River. THE ROANOKE RIVER ESTUARY The total area of the Roanoke River basin (pl. I) is 9.666 mi2 , the largest of any Nnrth Carolina estuary. However, only 3.506 mi2 of the drainage lies in North Carolina; the other 6,160 rni2 arc in southern Virginia. The Roanoke Ri\·er originates in the Valley and Ridge Province west of Roanoke, Va .. and flows in a general southeasterly direction toward the Atlantic Coast, empty- ing into Alhemarle Sound about 7 miles downstream from Plymouth, N.C. Principal tributaries include the Dan. Fal- ling, Otter, and Blackwater Rivers. The limit of lunar tide effects in the Roanoke River has not been well estah- lishcd, but is thought 10 be near Hamilton, about 60 miles upstream from the mouth. The gr_eatest width of the estuary, near the mouth, is only about 0.3 mile and-. upstream from Plymouth, widths are about 0. i mile or less. The narrow width of the Roanoke near the mouth is in sharp contrast to the_ Neuse, Pamlico, and Chowan Rivers which arc several miles wide at their mouths. The lower Roanoke, like the others are now, was once a drowned river valley. Now. how- ever, it has been largely filled by sediments. \Vithin the dClta thus fonned· is a fairly unusual system of dis- tributaries (fig. 4.24) which carry some water from the Roanoke into the Cashie River and, in the case of one large unnamed distributary, directly into Albemarle Sound. Maximum depths along the estuary vary from about 8 to 18 feet. A commercial navigation channel is maintained in the Roanoke River to Palmyra, 81 miles up- stream from the mouth. The channel is maintained to 12 feet deep and 150 feet wide from Albemarle Sound to about I mile upstream from Plymouth, a distance of 10 miles; thence a channel 8 feet deep and 80 feet wide to Palmyra, a distance of I 8 miles. Average annual precipitation over the basin is about 45 inches. The average annual outflow of the Roanoke River at the mouth is ahout 8.900 ft 3/s. second only to the outflow of the Cape Fear River among North Carolina ·s estuaries. Flow of the Roanoke River is highly regulated, par- ticularly by Roanoke Rapids Lake (details to be discussed later). The combination of relatively high outllow. small cross-sectional areas, and low-flow augmentation by Roanoke Rapids Lake. effectively blocks saline water 1 00 Hydrology of M;tjor Estuaries and Sounds of North Carolina from the estuary. During I 3 years (October 1954-Sep- tember 1967) of daily water sampling at Jamesville (sta. 0208 l 094 on pl. I). the maximum measured chloride con- centration was only 12 mg/L. Three .specific conductance surveys by the Geological Survey during normally low- now periods (October 6, 1954, July 25, 195,7. and Oc- tober I. 1957) failed lO reveal any significant saltwater en- croachment. even at the mouth. Significantly, the survey of October 6. 1954, \Vas made before increased low-flow augmentation from Roanoke Rapids Lake and at a time of record low strcamflows in many parts of the State. At that time, near maximum-of-record saltwater encroachments were being measured on other estuaries. ~hus, it is not lik~ly that any significant saltwat"er encroac_hmcnt will occur in the future in the Roanoke River estuary, even· under extreme drought conditions. as long as the current flow regulation patterns arc maintained. Flow Flow in the Roanoke River estuary has not been studied in detail: thus it is not really known what role winds play in the flow or to what· extent the flow. is af- fected by tides. We can infer that winds and tides play a lesser role here than in any other m:.Uor North Carolina es- tuary because of the relative narrowness of the channel and the lack of significant funneling effects. Conversely, we. can infer that freshwater discharges play a relatively larger role because of the greater magnitude Of the dis- charges in relation to channel cross-sectional areas. How- ever, validation of these inferences awaits confirmation from water-level records and flow measurements. As previously mentioned. the average annual out- flow of the Roanoke River at the mouth is about 8.900 ftJ/ s, or about 0.92 (fr'ts)/mi2. but average flows for a given year may range from about 0.50 io 1.50 (fr'ts)/m? (fig. 4.25). Actually, discussion of freshwater inflow to or out- flow from the Roanoke River estuary is not really mean- ingful except within the context of the existing patterns of flow regulation. Flow of the Roanoke River is extensively regulated by Philpott Lake, John H. Kerr Reservoir, Roanoke Rapids Lake, Leesville Lake, Lake Gaston, and Smith Mountain Lake. All of these reservoirs were created primarily for hydroelectric power generation. but many also provide for flood <..:ontrol, low-flow augmentation, water s.upply, and recreation. Because it is 1he most down• stream of these reservoirs, Roanoke Rapids Lake is most important from the point of view of its effects on flow in the Roanoke estuary. Pursuant to its license from the Fed- eral Power Commission, the Virginia Electric and Power Company must maintain, subject to special provisions. minimum instantaneous !low releases from Roanoke Rap- ids Lake (drainage area 8,395 mi2) according to the fol- lowing schedule: I iS(Fr:'S¥:r!7i1t· i1',1: ' --- .;f>t: -J··.- ;,..1 f~ · WINDSOR __\1,/_.J.'.-- .>I.(. •• ~ - --'1L .• ...JIL. zn ·:::rrn=1· F --"'--_..._ • ..:JL_ _,.,_ __ _.:.:.... J.: __ ......... -...'.U.. • ..I:.. _,JL.. -·---___ -.,..t_ ..-1{.. .JL .-->-IL...~°J,_ ~s--':; .- i,_:.: "--·-J:... -_i.k_ • -__ if_ __ _ --..,,v ___ _ ~-..'l'.... ~ -·-"'- r .L N . -..ill...: : • ~--•.;,_ • ...:.le'... ..>'.... -• -_ __:,J.,_ . ....:JL. ~ • ...IJL. ...!..!.... -..'1L -· ..'i::. -"'- "" 0 2 3 4 5 MILES 0 2 3 4 5 6 8 KILOMETERS ~--';, -~:-· Fig~re 4.24. Distributary system of the lower R.oclnoke River. -~-~--1\/ i11i11111111 ill.'i((ll/f(l/ll'(}l/5_ .flrm-. in_!i3/s . ~~-.January. F~bruary. i\·brch· .. 1.000 -~i~:~r;,,f n~r t~~~ '-',~_.\'O\'.cmbt:r. Dcccmht:r ........................ 1.000 I:::'~-Usually, actual releases from Roanoke Rapids Lake · !:,.exceed these minimum requirements. as indicated hy I ... eas~red nows of the Rrianoke River ·at Roanoke Rapids . ta: 02080500 in pl. I). Given he low. in cubic feet per __:~11_!~--arc estimated averngc monthly outflows ar the I ~10~th of the Roanoke River estuary for the period Oc- ·•~5r 1965-Scptember 1975. About 87 percent of these IP,o_w amounts are accounted for by· controlled releases 'om Roanoke Rapids Lake . ~-. ,. I January -····· 10,000 July 8,000 February. 12,000 August 7,500 March 10,000 September 6,500 April 11,000 October 6,500 May 10,000 November 7,500 June 8,500 December 8,300 The effects of high-flow fegulation arc reflected in the similar avCrages for January--May; flood flows are stored in the various reservoirs and released over long periods of time. Low-flow augmentation i.s apparent from the relatively high August-Noveriiber flows: they average about 0. 72 (ft3/s)/mi2 compared to only about 0.57 (ft3/s)/ mi:2 in the unregulated Chowan River estuary for the same months. Hydrology of the Albemarle Sound Estuarine System 101 = t or·., lllC1 NUS CORPORATION AND SI :· " CONTROL NO. DATE: July 19, 1990 REF. 30 TELECON NOTE TIME: 9:45 .. -~ 1-----------------''---------------''--------------i "l-" DISTRIBUTION: Georgia Pacific Hardwood Sawmill NCD00813 592 TDD No. F4-8909-89 ~ 11t fl 1-B_E_TW __ E_E_N_: _M_r_-L_o_n_g _______ ,-O_F_: _W_a_s_h-in_g_t_o_n_C_o_u_n_t_y_W_a_t_e_r __ r-P-H_O_N_E_:_(9_1_9_)_7_9-3--4-1_1_4 ____ -; Department AND: Louis McAdams, NUS Corporatio j: I It •' ·: ...... -. I . •• ·._· .~- ,. ••rk.:. ~---It .. ,. --~,._-_,.,. ,_ j:-· 1·· ft· • -· DISCUSSION: Subject: Extent of water service in the Plymouth area Service from Plymouth includes: East on N Oto Socona Church, east on Highway 64 past Macedonia to State Road 1319 to Pleasant Grove; south on ,ghway 32 to Sawyers Trailer Park approximately 0.5 mile from Morantack Road (south); west on Highway. Conni bay Creek Walkway is OfF' )lankin Lane in the city of Plymouth, Boy Scout Nature Trail sponsored by the city. No surface water intakes are located on the Roanoke at or east of the city, and none are on the Albemarle Sound that he recalls; the Sound is brackish and salt water. . ' ··il. ,:- \! ~ II REF. 31 }t ;; ; ::;;:1: :;[;;':~:!&, >;i;' ~;'J!ii: 'if i1§:;;;;;;;;;1':r1i'1i~'i{~';:l!:'1;~;1 ';~~t~l!~ ?':t':=:?:~f)t Reprint from North Caronna Administrative Code: 15A NCAC 28 .0313 Current through: February 1, 1993 ' lt' . I I D I I I i! I~ ,-·: '~· •--· 1--· 1.~ .. -1--~ \-·r ,··-1 I I ,·- ,. ' EHNR -ENVIRONMENTAL MANAGEMENT TISA: 02B .0300 SECTION .0300 -ASSIGNMEl\T OF STREAM CLASSIFICATIONS .0301 CLASSIFICATIONS: GENERAL (a) Schedule of Classifications. The classifications assigned to the waters of the State of North Carolina are set forth in the schedules of classifications and water quality standards assigned to the waters of the river basins of North Carolina, 15A NCAC 2B .0302 to .0317. These classifications are based upon the existing or contemplated best usage of the various streams and segments of streams in the basin, as determined through studies and evaluations and the holding of public hearings for consideration of the classifications proposed. (b) Stream Names. The names of the streams listed in the schedules of assigned classifications were taken as far as possible from United States Geological Survey topographic maps. Where topographic maps were unavailable, U.S. Corps of Engineers maps, U.S. Department of Agriculture soil maps, and North Carolina highway maps were used for the selection of stream names. (c) Classifications. The classifications assigned to the waters of North Carolina are denoted by the letters WS-l, WS-ll, WS-lll, WS-IV, WS-V, B, C, SA, ·sB, and SC in the column beaded "class." A brief explanation of the "best usage" for which the waters in each class must be protected is given as follows:· Fresh Waters Class WS-l: Class WS-1!: Class W S-Ill: Class WS-IV: f Class WS-V: Class B: Class C: Tidal Salt Waters 'Class SA: Class SB: Class SC: waters protected as water supplies which are in natural and undeveloped watersheds; point source discharges of treated wastewater are permitted pursuant to Rules .0104 and .0211 of this Subcbapter; local programs to control nonpoint source and stormwater discharge of pollution are required; suitable for all Class C uses; waters protected as water supplies which are generally in predominantly undeveloped watersheds; point source discharges of treated wastewater are permitted pursuant to Rules .0104 and .0211 of this Subcbapter; local programs to control nonpoint source and storm water discharge of pollution are required; suitable for all Class C uses; waters protected as water supplies which are generally in low to moderately developed watersheds; point source discharges of treated wastewater are permitted pursuant to Rules .0104 and .0211 of this Subcbapter; local programs· to control nonpoint source and storm water discharge of pollution are required; suitable for all Class C uses; waters protected as water supplies which are generally in moderately to highly developed watersheds; point source discharges of treated wastewater are permitted pursuant to Rules .0104 and .0211 of this Subchapter; local programs to control nonpoint source and storm water discharge of pollution are required; suitable for all Class C uses; waters protected as water supplies which are generally upstream and draining to Class WS-IV waters; no categorical restrictions on watershed development or treated wastewater discharges are required, however, the Commission or its designee may apply appropriate management requirements as deemed n=sary for the protection of downstream receiving waters (15A NCAC 2B .0203); suitable for all Class C uses; primary recreation and any other usage specified by the "C" classification; aquatic life propagation and survival, fishing, wildlife, secondary recreation, and agriculture. shellfishing for market purposes and any other usage specified by the "SB" and "SC" classification; primary recreation and any other usage specified by the "SC" classification; aquatic life propagation and survival, fishing, wildlife, and secondary recreation. NORTH CAROLINA ADMINISTRATIVE CODE 10122/92 i ·! I i fl I ,I ! I I I I • II II --:--. ,~ "!Ef:7J'iifr"11w;s:rew&Y!" .... .....--,;;• ---··2·0 r EHJ,R -ENVIRONMENTAL MANAGEHENT .0313 ROAJIOKE RIVER BASill Name of Stream Blue Hole Swamp !".atthew Slough Canal Gut Indian Creek Coniott Creek (Town Swamp) Frog Level Swamp Concho Creek Etheridge Swamp Beaverdam Creek fl.ill Branch Sweetwater Creek (Statons Pond) Hardison Hill Creek Long Creek Srr.i thwick Creek Ready Branch Dog Branch Conine Creek Devils Gut Gardners Creek Deep Run Swamp Lanier Swamp Copper Swamp ROANOKE RIVER BroJd Creek welch Creek Conaby Creek ALBEHARLE SOUND (Batchelor Bay) Eastmost River Eastmost River Cashie River Wahtom s.-amp Connaritsa Swamp White Oak Swamp Chlska Creek Description From source to Roanoke River From source to Blue Hole Swamp From source to Roanoke River From source to Roanoke River From source to Roanoke River From source to Coniott Creek From source to Roanoke River From source to Concho Creek From source to Concho Creek From source to Concho Creek From source to Roanoke River From source to Statons Pond, Sweet- water Creek From source to Hardison Mill Creek From source to Statons Pond, Sweet- water Creek From source to Statons Pond, Sweet- water Creek From source to Ready Branch From source to Roanoke River From source to Roanoke River From source to Devils Gut From source to Gardners Creek Frcxn source to Gardners Creek From source to Gardners Creek From 18 mile marker at Jamesville to Albemarle Sound (Batchelor Bay) From source to Roanoke River From source to Roanoke River From source to Roanoke River West of a line extending from a point of land on the southside of the mouth of Black Walnut Swamp in a southerly direction to a point of land on the eastside of the mouth of Roanoke River From Roanoke River to N.C. Hwy. 45 From N.C. Hwy. 45, including cutoff between Eastmost River and Middle River.to Albemarle Sound From source to a point 1. 0 mile up- stream from Bertie County SR 1500 From source to Cashie River F rcxn source to Cashie River From source to Cashie River From source to Cashie River 15 Class C C C C C C C C C C C C C C C C C C C C C C C Sw C Sw C Sw C Sw B Sw C Sw B Sw C Sw C Sw C Sw C Sw C Sw Classification Date Index No. 9/1/57 9/1/57 9/1/74 9/1/74 7/1/73 9/1/74 9/1/57 9/1/74 9/1/57 9/1/74 9/1/57 9/1/57 9/1/57 9/1/57 9/1/74 9/1/74 9/1/57 9/1/57 9/1/57 9/1/74 9/1/74 9/1/74 9/1/57 9/1/57 7/13/80 9/1/57 9/1/74 9/1/57 9/1/74 9/1/57 9/1/74 7/1/73 7/1/73 9/1/74 23-45 23-45-1 23-46 23-47 23-48 23-48-1 23-49 23-49-1 23-49-2 23-49-3 23-50 23-50-1 23-50-1-1 23-50-2 23-50-3 23-50-3-1 23-51 23-52 23-52-1 23-52-1-1 23-52-1-2 23-52-1-3 23-(53) 23-54 23-55 23-56 24 24-1-(1) 24-1-(2) 24-2-(1) 24-2-2 24-2-3 24-2-4 24-2-5 · 2B .0300 REF.32 1 North Carolina Inland Fishing, Hunting & Trapping Effective Jui'( 1, l8:.:l4 :o Ju:1e 30, Ff)r:; I I I I I I I I I I I I I I I ' LICENSE REQUIREMENTS AND INFORMATION ......... 4 FISHING REGULATIONS ............................................... 7 . Inland Game Fish .......................................................... 7 Warmwater Game Fish .................................................. 8 Mountain Trout ............. 9 Nongame Fish .............................. . .. 13 BOATING ACCESS REGULATIONS ............................ 17 HUNTING REGULATIONS ............................................ 19 Big Game .................................................................... 20 Small Game and Other Species .. : ............................... 24 Controlled Hunting Preserves.................. . ....... 24 Migratory Game Birds .................................................. 24 TRAPPING REGULATIONS ......................... . . .... , ...... 25 GAME LANDS REGULATIONS .. LOCAL LAWS ...... . Hun_ting and Trapping ............. . Local Fox Laws ....................... . . .. , ................. 26 ····················· 28 ···················· 28 ···················· 32 BIG GAME TAG REPORT ............................................ 33 UNLAyVFUL HARASSMENT ......................................... 33 APPLICATION FORMS .................................................. 37 Swan Permit Application .............................................. 37 Small Game Hunts Application .................................... 37 Trapping Application .................................................... 37 Wildlife in North Carolina Magazine ............................ 38 Managed Either-Sex Deer Hunts ........ : ........................ 39 Permit Turkey Hunts Application ................................ 41 Permit Waterfowl Hunts Application ........................... 41 Wildlile Endowment Fund ........................................... 42 Hunting, Trapping and Fishing are North Carolina's oldest and most cherished traditions. The future of these great outdoor sports depends on our wise and balanced management. We all must share in this responsibility. NORTH CAROLINA WILDLIFE CALENDAR To order the Calendar, or reserve your calendar for next year, please write: CALENDAR, NC Wildlile Resources Commis• sion, Archdale Building, 512 N. Salisbury Street, Raleigh, NC 27604-1188; (919) 662-4377. EQUAL OPPORTUNITY The Wildlife Resources Commission is an Equal Opportunity Employer and all wildlile programs are administered lor the· benefit of all North Carolina citizens without prejudice towards age, sex, race, religion, or national origin. Violations of this pledge may be reported to the Equal Employment Officer, Larry A. Campbell, Personnel Olficer, NC Wildlife Resources Com-· mission, 512 N. Salisbury Street, Raleigh, NC 27604-1188, telephone (919) 733·2241 . Cover photograph by Jim Dean of the North Carolina Wildlile Resources Commission. "The publication ol this digest was paid lor through the sale of advertis(ng. The North Carolina Wildlile Resources Com- mission neither endorses products or services listed nor accepts any liability arising from the use of products· or services listed." Published by WJF Marketing, Inc., Lebanon, Oregon 97355. For Advertising inlormation call Richard Meyers, Advertising Sales Manager. Phone 503·259-2991. State of North Carolina James B. Hunt Jr., Governor Department of Environment, Health and Natural Resources Jonathan B. Howes, Secretary NORTH CAROLINA WILDLIFE RESOURCES COMMISSION John F. Lentz, Chairman.: .................................. Ellerbe Bobby N. Setzer, Vice Chairman ................... Cullawhee Susan L. Allen ............. :. . ................ Cary Richard P. Budd .. Winston-Salem Ovide E. de St. Aubin .. . .............. Siler City Junicr W. Dew. .. ...... Hallsboro Lawrence "Larry" Diedrick ..... . ........ Rocky Mount Russell M. Hull, Jr. .. Elizabeth City Ted B. Lockerman ........... Clinton John W. Parks Ill.. . ........... Gastonia John E. Pechmann. . ...... Fayetteville Roy Gerodd Sowers 111.......................... . ......... Burgaw Jerry W. Wright.... . .......... Jarvisburg Charles R. Fullwood, Executive Director Raleigh FOR ADDITIONAL INFORMATION, CONTACT: North Carolina Wildlile Resources Commission 512 N. Salisbury Street Raleigh, NC 27604-1188 For motorboat registration call 1-(919)-662-4373 For license information call 1-(919)-662-4370 550,000 copies ol this public document were printed at a cost of $48,519 or $0.08 per copy. gill nets in the Northeast Cape Fear River and Long Creek; with dip and bow nets in Slack River: and with seines in the main run of North-east Cape Fear River. December I-May I with gill nets in Black River: and with dip, bow. and gill nets in Moore's Creek approximately one mile upstream to New /.toon Fishing Camp. Perquimans: July 1-June 30 with traps in all inland waters. December 1-June 5with dip and bow nets in all inland public waters. excluding public lakes, ponds, and other impounded waters: and wuh gill nets in all inland public waters. Person: July I-August 31 with seines in Hyco Creek and Mayo Creek. July 1 -June 30 with gigs in all public waters. · Pitt: July t .June 30with traps in Neuse River and in Tar River below the mouth of Hardee Creek east of Greenville. December I-June 5 with dip, bow, and drift gill nets and with seines in Tar River; and with dip, bow, and gill nets in al! other inland public waters, except Grindle Creek, and Contentnea Creek berween NC 118 bridge at Grifton and the Neuse River. Polk: July f.June 30with gigs in all public waters, except designated public mountain trout waters. Randolph: December 1 -March 1 with gill nets in Deep River and Uwharrie River. . July I-August 31 with seines ·1n Deep River above the Coleridge Dam and in Uwharrie River. July (-June 30with gigs in all public waters. Richmond: July I-August 31 with seines in all running public waters. except Pee Dee River from Blewett Falls Dam downstream to the Seaboard Coastline Railroad trestle. July f ·June 30 with traps and gigs in all public waters, except fakes located on the Sandhills Game land. December 1 • June 5 with dip and OOw nets in Pee Dee River below Blewett Falls Dam; and with gill nets in Pee Dee River below the mouth of Canledges Creek. Robeson: December I-March 1 with giH nets and gigs in all inland public waters. Rockingham: July 1-August 31 with seines in Dan River and Haw Rivar. July I-June 30with traps in Dan River; and with gigs in all public waters. Rowan: July 1-AuguSt 31 with seines in all run-ning public waters. July 1. June 30with traps and gigs in aU public waters. Rutherford: July 1-Augusr 31 with seines in all running public waters, except designated public mountain trout waters. July I.June 30with traps, gigs, and spear guns. in all publ'1c waters. except designated public mountain trout waters. Samp.::ion: December I-March 1 with gill nets in all inland public waters. December 1-May 1 with gill nets in Big Coharrie Creek, Black River, and Six Runs Creek. May 2.June 5 with gill nets of no less than 5½-inch stretch ·measure in Big Coharrie Creek, Black River, and Six Runs Creek. December 1.June5with dip and bow nets in Big Coharrie Creek, Black. River, and Six Runs Creek. Scotland: December I-March 1 with gill nets in all inland public waters except lakes located on the Sandhills Game land. Stanly: July 1-August 31 with seines in al! runriing public waters, except Pee Dee River between Tillery Dam and Rocky River. July 1-June 30 with traps and gigs in all public waters. Stokes: July I .June 30 with traps and gigs in all public waters, except designated public moun-tain trout wators; and traps may not be used in Belews Creek Reservoir. Surry: July I-June 30 'Mth gigs in all public waters, except designated p.;blic mountain trout waters; and with traps in the main stem of Yadkin River. Below is a listing of current fish consumption advisories tor North Carolina waters: Body of Water Advisory Pol\utaot Hyco lake and All Fish. No consumpbon by women· of child boaring age. Selenium Be!ews Lake No more than 4-6 ounces per week tor the general Albemarle Sound (from Bull Bay to Harvey Point west to mouth of Roanoke and Chowan fr,ers) Roanoke River (Hwy 17 in William- ston to the mouth of Albemarle Sound) Chowon River (entire river in ,·~CJ Welch Creak (Martin Co.} Pigeon River Pages lake, Pit Links and Watsan lake (Moore Co.) 8"19 Creek (Columbus Co.) Waccamaw Rlvr:r \Columbus ano (Brun~wicl-. cos.; 16 population. All fish except herring, shad and shelf fish. No cons-umption by pregnant women, nursing women and children. No more tha~ two meals por month for general population. All lfsh except, herring, .::ihad and shellfish. No cons-umption by pregnant women, nursing women and children. No more than two meals per month for general population. All fish except, herring, shad and .::ihellfish. No cons-umption by pregnant women, nursing women and children. No more than tv-to meals per month for genera! population. Al! fish except, herring, shad and :.hellflsh. No cons-umption. All fish. No consumption Largemouth bass. No consumption by women of child-bearing age and children. No more than two meals per month lor the general population. Largemouth bass end bowfln (blackfl.::ih). No cons• umption by women of childbearing age and children. No more than two f"l'"ll:!.:ils per month for the goneral popul;ition. Dioxins Dioxins Dioxins Dioxins Dioxins Mercury Mercury Swain: July I-June 30 with gigs in a/I public waters, except designa led public mountain lrou{ waters. Transylvan!a: July I-June 30 with gigs in all public waters. except designated public moun-tain trout waters. Tyrrell: July I-June 30with traps in Scuppernong River and Alligator Creek. December 1-June Swith dip and bow nets in a!I inland public waters, excluding impounded pub-lic waters and Bee Tree Canal within 50 yards of the lake Phelps fish ladder. December I-June 5·with gill nets in Alligator Creek. Union: July I -August 31 with seines in all running public waters. July I-June 30 with ll'aps and gigs in all public waters. Vance: December I-March 1 with gill nets in Southerlands Pond and Ellis Pond. July 1-Augus/ 31 with seines in the Tar River. July 1 .June 30 with gigs in all public waters, except Rolands. Faulk.ners, Southerlands, and Weldon ponds, City lake, and Kerr Reservoir. July I .June 30 with dip nets ln Kerr Reservoir. July I .June 30withcast nets in all public waters. Wake: July I-June 30 with gigs in all public waters, except Sunset, Benson. Wheeler, Ra-leigh, and Johnson Jakes. December I •June 5with dip and bow nets in the Neuse River below Mi!burnie Dam, and Swift Creek below Lake Benson Dam. Warren: July I-August 3T with seines in Fishing Creek, Shocco Creek, and Walker Creek: ex-cluding Duck and Hammes Mill ponds. July I-June 30 with gigs in all public waters, except Duck and Hammes Mill ponds, Kerr Reservoir, and Gaston Reservoir. July 1-June 30 with dip nets in Kerr Reservoir and Gaston Reservoir. July I-June JO with cast nets in all public waters. Washington: December 1-June 5 with dip and bow nets in all inland public ',Yaters, excluding impounded public waters; and with gill nets in Conaby Creek. Wayne: December 1·March 1 with gill nets in Sasser's Mill Pond and Sleepy Creek Lake. December f-June 5 with dip and bow nets in Unle River. Mill Creek, and Neu so River, except from Quaker Nee~. Dam downstream to SR 1008 (Tolar) bridge. Wilkes: July 1-June 30 with traps in Yadkin River below W. Kerr Seen Reservoir; and with gigs and spear guns in a!I public waters, except designated public mountain trout wa!ers. WIison: July I-June 30 with gigs in Contcntnea Creek (except Buckhorn Reservoir), including unnamed tributaries between Flowers Mill and SR 1163 (Deans) bridge. December I-June 5 with dip and bow nets in Contentnea Creek below US 301 bridge and in Toisnot Swamp downstream from the La',,;,e T oisnot Dam. January I-March 1 with gill nets in Silver lake. Yadkin: July I-June 30 with gigs in all public waters; and with traps in tho m;;iin stem of Yadkin River. . Tu~~~!ifi~&·~wws e-~~ J~M ... · ... ~=,,=-~-"~ . ·'s:i t~!N1?€> R ~~iJHJ~.~ .. ,""-.•,t POSSESSION OF CERTAIN FISHES It is unlawful to :r:;r,'.3D')rt, purchase. pos5GSS, or sell nny species ol p11~nhn, !hrJ "walking cat1ish· (Clnrias b.1lrachu:;;_ ":of 1h,:: ·11hi1n :1mur or ·grass REF. 33 Cl Cl 1990 Update Fish Tissue Dioxin Levels in North Carolina North Carolina Division of Environmental Management Water Quality Section 1!1fi f~i.:-~· : -ir.- t 'fr'"• ~i¾·,, li:~~·~t· I~,,,,..,. "···.:- i\t,i-' .:i,'~, Introduction 1990 Update Fish Tissue Dioxin Levels in North Carolina l ti.::'1;:. I i; Dioxin has accumulated in fish found in the receiving waters of pulp and paper \J •• -t~ • 1'fi;''~ facility effluents. Elevated levels of dioxin found in fish during 1989 sampling I~~f~-prompt:d the Sta~e Health 1:)irector to issue ~everal fish co~sumption advis?ri~s i -;~;,~ (listed m Appendix C). This report summarizes the analytical results of dioxin i",{: measured in fish tissue with emphasis on results from 1990 collections. All ~:; available data, whether collected by the Environmental Protection Agency (EPA), li-z7-· the Division of Environmental Management (DEM), or the pulp and paper ,~;, industry, are inclu~ed in Appendix A. The ~~"". informa~ion ~resented within this ~:; :· summary report will be evaluated by the Divis10n of Ep1dem10logy and the State I:;~'. Health Director. This evaluation will determine if dioxin fish consumption ~~-' advisories for the recreational and commercial harvest of fish require modification. ·1 The Division of Marine Fisheries and the Wildlife Resources Commission will le·· likely receive recommendations from the State Health Director based on this risk . assessment evaluation. The Wildlife Resources Commission and the Division of I•·•:' · Marine Fisheries are responsible for regulatory and fisheries management decisions ·. on consumption advisories. .-.·,J: I.;..,..,. ~~ -=~ ,~:~ I-·~:.: ~~-,i,-. ••'-. I'"\_:-~:..:·:· -<; •• , .. r·. 1-.;.;_,, :~· t:· i"•F·: ..,.;. f-~-.. i-i:/· ~--,. :;.!""-• -::· ...... ·•.· . ...... ' ·,,- -~-~ i~-· , ... _, Background information on dioxin contamination and the facilities required to test fish tissue are included. Also included is a brief summary of past work and the rationale for testing in 1990. Site selection, species tested, and analytical methods were chosen after careful consideration of data needs and lengthy discussions with the Division of Epidemiology, Division of Marine Fisheries, and the Wildlife Resources Commission. The 1990 spatial extent of sampling varied tremel\dously due to the location of pulp and paper facilities and the nature of the receiving waters. Background Polychlorinated dibenzofurans (PCDF's) and polychlorinated dibenzo-p-dioxins (PCDD's) are two groups of compounds composed of 135 and 75 individual isomers respectively. Some of these isomers are toxic at extremely low levels, particularly those with chlorine substitutes in the 2,3,7,8 positions. This collective group of 210 individual isomers is commonly refered to as dioxin. The formation of 2,3,7,8-tetrachlorodibenzo-p-dioxin (TCDD) and 2,3,7,8-tetrachlorodibenzofuran :. (TCDF) in the bleaching of certain pulp material and the discharge of TCDD and TCDF from pulp and paper mills has been well documented.· : The Environmental Protection Agency (EPA) initiated nationwide studies to determine if fish tissue had been contaminated by dioxins and furans. Results of these studies in North Carolina revealed dioxin fish con.tamination near pulp and paper facilities that used a bleaching process. Under the authority of Section 308 of the Clean Water Act, administration of surface water discharge permits (NPDES) and North Carolina General Statutes §143-215.3, the Division of Environmental Management required pulp and paper facilities to assess dioxin contamination in fish and/ or shellfish tissue in effluent receiving streams. · - " I i' I i I I I, I. \I ' I I f I ' 1· I I :~ I I I I I I I I I I I I I I I·; . I ' ; ~- The following is a list of pulp and paper facilities discharging to North Carolina surface waters (Locations shown in Figure 1) : Facilitv Champion Paper Weyerhaeuser Weyerhaeuser Ecusta, P.H. Glatfelter Alpha Cellulose Federal Paperboard Union Camp Location Canton Plymouth New Bern Asheville Lumberton Riegel wood Virginia Receiving: System Pigeon River Roanoke River Neuse River French Broad River Lumber River Cape Fear River Chowan River Given concern by the public, industry, and government agencies, this summary is intended to provide new individual fish tissue monitoring data from the above facilities and from agency monitoring activities. It is further intended to composite all fish tissue information on dioxin into one summary document available to all interested parties. Summarized results of all dioxin fish tissue monitoring in North Carolina performed by industry, DEM and EPA are included in Appendix A. Laboratory support for these results was made available by EPA, the Albemarle Pamlico Estuarine Study (APES), and by individual pulp and p';Per industries. · · Figure 1. Pulp and Paper Facilities in North Carolina ALPHA CELLULOSE FEDERAL P.APER EOARD . ~~ . ,;..';J -·;1r ,-I~ jj -.;1:f.J .. ti Historical Studies and the 1990 Approach :,ll'.j'~ Dioxin in fish tissue was first sampled by DEM in 1984 as part of the National .:.:_~ Dioxin Study. Sample locations were selected as background sites to determine if ~~1~0 • · 2,3,7,8-TCDD ~as ubi~uitous in t~e aquatic envi~o.nmen~. In the spring of 1987, ,,:-~"~ .. under the Nat10nal B10accumulat10n Study, additional isomers were evaluated. :-"Ajf. · Site selection included three contaminated sites and one background site. All four 'i<i~Jfiii sites had detectable levels of dioxin. These results revealed concerns for fish tissue :~tl , contamination below pulp and paper facilities using a bleaching process in North /.:.'r:!i.f~.1 Carolina. To further investigate this issue, fish tissue samples were collected ~f~-1/·~ be_low fiv~ pulp and paper mills during the winter of 19871_88 _and below two o~er ~Ji:i~-· mills durmg the summer of 1988. Detectable le_vels of d1oxm were found at all ;:ci!o'' seven locations. Additional sampling oc~urred m 1989 as part of the Albe~a~le if;{f:~ Pamlico Estuarine Study (APES). These sites also had detectable levels of d10xm.~{t,·· . · . ;:=tf ,I .i '--. . ,rl4 ' ____ .,,_,., ... rrt::- ~t~·,.::~--•' I -~;";.,. ' y•"::-·~ •' As a result of this information and the needs of the Division of Epidemiology to evaluate public health concerns, bleached pulp and paper industries were required to perform assessments of fish tissue in effluent receiving streams in 1990. Concurrent with this effort by industry, the Division of Environmental . Management, assisted by the Division of Marine Fisheries and the Wildlife :tL.:.:: ':j"• -• I •• "f""_v.i-·{' . •:' Resources Commission, conducted additional evaluations to determine the spatial ··extent of dioxin contamination in fish tissue. .-:,,:.. .f:, Based on the information obtained from 1984 through 1989, the Division of r Environmental Management elected to focus 1990 fish tissue monitoring efforts ·,--ac--on 2,3,7,8-TCDD and 2,3,7,8-TCDF. This decision was based on the composition of .. ,,___ dioxin isomers encountered in previous sampling and the toxicity eqilivalency ·/ ~i-~-----. factor (TEQ) rating of these isomers. The TEQ value is calculated assuming ·· ~:l•--: . additivity of effects from individual cogeners of dioxins and furans and is ~··• · expressed as an "equivalent amount of 2,3,7,8-TCDD." The basis for this approach ·---· is to aid in the assessment of the human health risks posed by mixtures of dioxins and furans since the bulk of toxicological research has been performed on the ; ;: · · TCDD cogener. Thus, by combining the TEQ approach with the toxicology •'· ."---information available on TCDD, the risks associated with consumption of a -~ ;:.: ..... mixture of dioxins and furans in fish tissue can be estimated. Dioxin cogener ! information obtained from 1984 through 1989 indicated, that on the average, i :;.f·•: _____ TCDD and TCDF laboratory analysis provided greater than 90% of the dioxin ' F.: information necessary to calculate the total toxicity equivalency value (TEQ)l. The :"[f]; -90% return of information and cost efficiency in analyses suggested benefits in i ,;~J::,i, performing 2,3,7,8-TCDD and 2,3,7,8-TCDF analysis only. Laboratory identification '\k ·: of additional isomers is quite expensive and provides little additional ~c/t-~ information. Therefore, the new information available within this summary 1''.',rLT. reflects the most cost effective and timely acquisition of dioxin data from all i..L. . ;:ti·;:· . available sources by _focusing measurements on 2,3,7,8-T~J:?1? and 2,3?,~-TCDF. !lr.~:... Furthermore, composite samples were analyzed, thus max1m1zmg the eff1aency of ·/,.:.-~; la,9oratory costs and providing information from a large number of fish . .: ! c.,.' i-·;_;;-t· . rrr~ i ., t:.:~~ . ·rr·· :·' j!,;:~ .. '· ,,...:...... . r ~~ . ) ............. ·I •I . r-:-· tr--:7""· t4Jt;~. -· . ,, . . -: . !T?-;-. f-,•--··-... ·;{£~- 't .... --: ' ·-". ;-·~-----~ -- 1---·-lNorth Carolina Division of Environmental Management, Water Quality Section. (1990) Fish Tissue Dioxin Levels in North Carolina. 3 33 Summary at Individual Dio~in Fish Ta.sue Samples 2.67 :711 ''ji ·s Wal::n Cr at old Wevert,nu5Gr discharnca Mav 2'3·June 5. 1990 Pumol<.inseed till,1111 86 ,.s· 3.8 7.8 P 11 s wc.i:n Cr at old w, .... muuser dischar0et June S·Seot 27. 1990 White Carlish lillel/5 362 s.,· 6.1 2.7 ~ r, s Welch C1 at old w,.,.muus.er d.scharov June S•Seot 27. 1990 Whne Cat!~h tille\/5 362 6.5"/duol 6.2 3.4 ..:...., 'tt s Welch Cr at old Weverhaeuser discharoa S•Jun-90 Whi11 Catfish lille\/1 2213 5.5" 5.3 1.11 f-AR0Jr:ok,Ri ..... 1•tPlvmouth 10111190 B!ueCral:I meat/18 e.o· 3.1 29 ~ lo A Roanoke River nur Weyerhaeuser discharge 12120188 Laro-mouth Bus lill11l5 1387 23.2 17,612 55.~ ,f 1o •S Roanoi<.1 River near Wevertluuur discharc:a AnrillMav 1989 White Cat!ish Fillel/8 125 28.2 21.507 • 36.835 ~ lo s RoJnoke River near Weverhaeuser discharoe Aoril/M ■ v 1989 Blueoill Fillet/• 128 18.5 17.981 •.529 ::-10 S Rolf\(ll';e River roe■r Woverhaausor disehame AQ11llM1" 1989 Bluenilt Fillel/8 57 18.2 17.329 a.20, "ti s w1t:h Cr 11 old Wovemaeuser discnaroe 23-Mav-90 Laroemouth Bass lille!/4 3'-8 5.0" 4..6 3.5 2. 18 2.46 3.54 1.85 t I :~ ! :::~:: ::::; ::; ::::::~::; ::;~:;: :::::;~:; ~::: ~~1:w c:e~:: ~:::::;: 1 5 1~ 1\ !:;:! ;::~;; -tO S Roanoi<.e River near Weverhaeusor diseharoe _..,.ril/Ma" 1989 Gizzard Shad Whole/2 273 -0.5 t0 0.773 .:_ ~ ~ ;:::;-ddla Ri,,er al NC 4.5 5/2189 Laraemouth Bass lille113 4.33 9,5 9.1 3.2 ~ 11 A ri\1(.ldle Aiver at NC •5 512189 Channel Catlish tillot/3 1620 9•.2 77.7 1'7 .~ 12 A Albomarle Snd@ Terragin Pt 512/89 Lar mouth Bass !illet/3 924. 8.1 7.107 9.687 1_ I 13 S Roanoke Rivor at Marker 15 Alldl/Mav 1989 White Catfish Fille\/6 370 U.6 11.981 19.068 +-13 S Roanoke River at Markor 15 Aoril/Mav 1989 White Catlish Fillet/6 370 1'.1/duoJ 11.394 19.11 :.!_ fl S Roanoko River at Marker 15 April/May 1989 White Catfish Fillet/4 203 18.9 12.177 29.945 ·•· .._ "!j.. 13 S Roanoke River at Marker 15 AorillMav 1989 Bluellill Fillet/7 4.2 16.9 1".799 20.531 :!._ l-,c,'-r.s;-1:Rs,:',::oo::c,,:-cac;,:,::,-:,::,-;M;,::,c,,:',c,;15;-----------t- - , ; , : ' : , ' s ; , c , M ' ; , : c . , : : - , c , c , o , ' - f o a ' c , , : ' , ' - : : : Q ; C 1 1 - - - - - t - a , s ; , ; : , , ; ; , ' ; , ; , - - t - - - - , , ' a , ' - - t - - - - ' - ; , ' - ' - - - t - - - ; , ; ' . ~ , , . , , ' - - t - ' ; , ; - , ; ' , ; ' , ; - - t - - - l +-13 S Roanoke River at Marker 15 Anril/May 1989 Black Crappie Fillet/4 92 21 19."45 14.563 j ,•,.f ;.:_ 13 S Roanoke River at Marker 15 Aoril/Mav 1989 Blaci<. Craonie Fillet!'-233 27.6 25.135 24..668 !. 13 s Ro,oo'-a,,.," M"'" 15 Ao<11/Ma, \989 Bl•" C,ao,;, F;11,.,, 233 36.9/deo\ 3',1'7 27.•2' I •\ 13 S Roanoke River at Marker 15 Aoril/Mav 1989 Yo!\ow Porch Filletl:l 54 16.3 10.289 59.015 :: I 63 S Rolnoke Rivor at Marker 15 10/2/89 Blueoill Fillet/7 86.7 20.8" 16.6 42 ••· 13 S Roanoko River at Marker 15 Sept 27.29.1989 Black Craooie Fillet/4 140 ,.8· 3.6 11.8 '.i;~ 63 S Roanoke River at Marker 15 Sent 27.29.0ct4 1989 Channel Catlish Fil\o\/3 538 43. 7" "1.2 24.6 · f! ., s ""~"• a;,.,"""'" ,s s,,. 1'-13, ,,.o a1,c1, c~oo• 1;11.,,s m u· o.a, ,.s 2.ss I , 63 S Roanoke River al Marker 15 Sept 11-13. 1990 Channel Cat1ish lil!1115 14.09 26.4" 26 3.8 2.56 .. ·.~ 63 S Roanoko River at Markar 15 Soot 11-12, 1990 Laro.mouth Bass tillet/B 361 2.'-" 1.7 6.9 2.16 _;_ 63 S RoanokoRiveratMarket15 Soot 11-12, 1990 LaroemouthBass lillot/8 361 1.9"(duo! 1.5 '-'i:;··r,• .=.,_': I :: , S Ro:lnoke River at Marker 15 Sent 11·13. 1990 Whito Catlish liltet/5 396 8.0· 8 NDtO.U\ •2.66 , ,t-"--+",'·+RoJnoke River at Sans Souci 5/2/89 Lar011mouth Bass 1illet/1 675 10.8 10.326 4..192 I:~ ; "-:=•~·~=t=•~~~a:00r00~1-1,Ja;;,~.~·=•r•J 5~•~01•J•~0~,~,t; ================1:::::1,'.:12t10•t•t=====~'~"~'" ~ ... ~mj,~,j'"::;a~.~ .. ~==t=:I1t11t1ot,t,:;,::j::t,~•2°::t::::j,~,j.,t::::1:::j,j,~ .• t~==t:::'.),t,t~::1:::::j -64 A Rolnoke River at Sans Souci 512189 Redoar l!llot/2 4.50 6.7 B.l 6.6 -54 A ReJnok11Rivera1SansSouei 12/20/86 LaroomouthBass lillot/5 530 29 27.112 19.299 '•).~ .:::::;,. I t-'c'~+-'A'-+=R•"cOO.cc,'•'c"c;, ••• ,c•o•cS.c"',"'"s","""'"; --------+---c'""''"'"''---1''"""'" ="m"'"""'"'-" .. "''''--+-"' 'c'c"c'c'.,'-+-"'"'"'-1----''"'"· ''----+--',""'"'"''--+-"'•·•"•''---+---l ; ~~: ii"' 65 A Roanoke River at Moutn 512189 La1~mouth Bass fillot/1 1008 9.1 8.709 3.171 64 A RoJnoka River at Sans Souci 512189 Laroemouth Basa li!let/5 34.2 24 23.8 2.3 .1,.··iD·. ,•, -65 A Ao~noke River at Mouth 512/69 Whrt1 Best lillet11 575 0.9 EMPC(1.3) 8.2 -65 A Roanoke River at Mouth 5/2189 Laroemouth Bass lillot/1 850 10.7 9.4. 12 -=lrc';;'c-r''-f"=--"'"00=c;'c'c"c;'c'c'c'o'c"c'"""""-----------+---"'"""-'"'"''---ll''"""'~=•mcP o " c " : _ , ; a , e , c • c _ - t - c ' ; c 1c1•c•c1c'-+-'-'"'"'-1----''"'"''---+--'-""'''"'--+-"'"·s"c''---+----1 ~'' 65 A Rc3noke River at Mouth 512/69 Lar011mou1h Bass lillot/6 420 12.0 11.7 2.7 ... ,;! 66 S Casr.ie River 11 Windsor SeD! 19-20, 1990 Blaci<. Crao::,ie tillet/2 310 o· ND(0.161 N0(0.25) 3.'-3 -66 S Casnie River at Wind50r Oct 6-7, 1990 Channel Catt1sh lille\/2 2592 1.6" 1.6 ND(0.26l 3.42 -66 S Casnie Ri~er at Windsor Sect 20•0ct 7. 1990 Laroemouth Bass lill11119 726.5 o • ND(0.041 0.08 4.43 ~1:a::,,',· 11 S6 S Casnoe River at Windsor Sept 19-0ct 7. 1990 Yellow Bullhead fillot/6 ~93 o· ND!0.05l ND!0.251 2.53 fj1 .:=J,, ,: .. ~ •,:,' S C3sr.ie R;ver a! San Souci Ferrv 19·Seo•90 Channel C;i:1isn 1illet11 5033 o· ND(0.321 ND(0.74l J.e6 ■-. S C.:sr.1e River at San Souci Ferrv Sept 19·20, 1990 Channel CJ111sn lillet/10 2004 1.4• 1.4 N0(0.451 5.05 -; 67 S CJi~,e River at San Souci Ferrv 16-Seo-90 La1Q11mouth Bas, tillet/11 366 O • N0/0.41/ ND(0.59) 2.66 · ,--:,a,c-t-'s'-+c"",.",",ie'-"s";,",",",","s",","s",",",";",".,",~'------- - + ~ s - , - , " , " , " , " . , " a " , = . , - , - , - 1 ! ' , " . , " " o , , " m " , ' , " . , ' " ' a " . , ' , ' - - + ~ " , ; " 1 " 1 , " , " , " , ' - + - , " , ' , ' , - l - - - - ' , ' - . - - - + - N " ° ' o " 1 , o " . 2 " , , " - + - ' N " o " , " a " , " , " , - + ~ c , o , - - i ~:· -, ·=j•~•L=tj5t!Atl~bio~m~a~•"~j5o~~"~"'~j•~•jM~•~'f'~"ti'::::::::::::::::t:] 5~'~'t' j'j'~''b't':'t•~•~'[j~C~h~•~'°~•~IJCt•~•ilifis~ht:::t:j'±;'ti'~'f"d'd't: j : = • Q • ~ • ~ • t : t : : I ~ • ~ • = · ~ ' ~ • ~ l = = ± = = = ] 1 ' = ' L : : : t : : : j ' j · ' t : : : t : ~ ' ; · ' ~ ' = ~ ,f'&i IS = ; 6 6 8 8 S Al!:J~marle Sound at Marker 1 Seo1 11-13, 1990 Channel Catlish lillet/10 1656 21.5"!duc\ 21.1 4.3 I" -;';--tc5~oA1ebs•cme•"'"'-'So,ee"e""e..,•e•c•c•e•!••e•ec.'---------t-~Se•e"'-''>'c·>cJ,,_c < 9~9~0'-i~Cche•e0°C•e1cCs•c•fl;eshc__!-_cl;"lel•c•e1•7_+.-'c5C2e9c..,!---'C0c·c'~·---t--09c•c7 __ !-_03C8'--f-,3c'~',1 -·~•c•c..+sS..i,Ae,lb!marle Sound at Marker 1 Seot 11·13, 1990 Lar011mouth Bau li\le\/3 367 1.8" 1.2 6.'-3."9 -68 S Alb11marle Sound ,t Matker 1 5101 12-21, 1990 Whrto P•rch !ille!/12 154 7.9" 5.1 28 2.a, -:J:;.': -= I GS I S Blackwater R, 15 mi UPS Union Camp dischar~• Sect/Oct 1989 Larnamouth Bass Fillet O • NDI0.91 0.21 :Jr• 69 s B~:kWl!lf R. 100 15 mi UPS Union Camo discham• Aue/Sept 1989 B\uea1II F;llet O. N0(0.7l 0.29 11·~ ; 69 S Bl3ckwattf R, 1op 15 mi UPS Union Came disct,arn• Aun 18•25 1989 Ch1nn1I Catlisn Fillet 2.3" 2.3 N0{0.1el ~• -1 6S S g1:i:kwa1er R, a.,o 15 mi UPS Union Camo discna1 March 8·13.1990 Lar011mouth Sus Fille1 o• ND{0.5) ND(0.3) , -1 69 S Blackw1t11r R, aoo 15 mi UPS Union Camp dis.enar"• March 8·13.1990 Blueoill Fillet O • ND!0.191 ND(O.tll -= I ~9 S Blackwater R 100 15 mi UPS Union Camo discharn• 2113190 Channel Catlish Fillet ,.o· 3.9 1.33 ,..,. ~' ~·~•;_+~·-M•~1,~,,,.,.~·••c'~"'-'"'£"i!J'~'Jm,!'..; gu~P~SJU,!a~;~o,~C::•~m~p~d~;~£"!'!!"~'---'e'c'G'~'~•~''--. . J ! C ~ h ~ • ~ ' ~ " ! ' L . f C ' ; • ~ " ~ " ! ! h _ _j_~w~"'~'·'--:I---..J.--l'c•!':· __ .J.._-2.0J.8l__,l.-_~o~.2~J'--t,, .. ,..-i. c' ~·~•;_,1..•e.j~•~"c'!'••·~•!•c• B"!2'£"i!J'2'Jm,!'..; ~UfP§SJU,!a~;p~a~C::•~m~p~d~;~~"'!'!!'"i''!i--...c'!'c'Ll'~'~•~ o , _ _ _/JB~l~"'~'~·~"'~":'c•~rr~•e"L-l--'D~,a~wcac__Ji----l.--J•~•:· __ .J.. _ _!•J.2'---1--~'!;'~'--t-;~H . -I' .... 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J . . - ~ i · 1~1!''--II---..J.--~'c.e:· __ .J.. __ .!.l''---l---,,~~~b;;--!--::Jl1.t_ ',' 1 S Blackwater A. aDP 5 mi UPS Union Camp di$Charoe ~ ·4 ~I : lr1 .:t;i:::t1!tt:i:~:l:~,:~:~:1::~:i:1~:~·~0000ij~:;_"~:ii:i~~:~:tt~~;Tu;:~;jc"0l:::~"'~,~J..':~::c~,1:~:~:~:•~'--ir_-:_-_-J~~!:~,~bt:1:1:~::::i'~ l . ~ · ~ : ~ • c ; ! ~ s i h h ' _ : : : : : : : : 1 t : : ] ,0'J;~:~:~:~::::i::::::i:::},j,,~'.i,~.~;~,;j_,:::t:::2;t•!:,-:_-_-~_-_~N ~ N ~ ~ t , ' ~ i • * ; r : ~ · , : : . i t : : : : j J I ~ -\ 1l:?'i"~--"f_~•t1-~•~'';;'f"~•f•~•..:•~•~~"~·1•~=~1 5J~mf[;tu~P~sJ~uf'f;~o~,~~Ct•7imt't1•~•~•~c~h~•~•~"~•~t:: - - : 1 ' ~ ' ! ' ~ ' ~ ' J 2t·.!.';j'f'l'j'~•f9i:"::-~gc~~h~•7i'~'~'~'r~c1~~•~;~,~h~::i:~JF~;~,~'!•i•c'~'t:1t:::::: i : : : , : 1 ' ~ · 1 ' ~ - E . L : : i : : : : i ' j · ' t - : _ : : i : : : j ' ~ ' ~ ' t : : 1 : : : ; ; ~ ~ if- 7 7 0 0 S Bl~ckwa1er R app 5 mi UPS Union Camp d1scharo11 Mav 2·12.19S9 Channel Catfo1h Fillet/3 1,5·tducl 1.5 0.35 ''.= 1'!'1 S BIJCkwa1erR aoo5miUPSUnionCampdischarce Mav 2·12.19S9 Channel Cattish Whole/Como 1 '-" 1.'-o.39 •-1:!r I ·L 70 IS Bl:1:,,,.,a111 R aoo 5 mi UPS Union Camo discharne May 2·12.1989 Channel CJ\\i~~ Whol11Comn 1.6" 1.6 0.'-6 ,' :~ /I~,~ .\!-~s - ---~~~ ffl . I lj s. Industry Monitored, A-Agency ND-non-detected EMPC-Estimated Maximum Po1ential Concentra1ion .. .a...w -~·.tf • ,~(Roanoke River System ltilsampling locations are shown in Figures 2 and 5) l,~;.~~ish s~mples were collected to evaluate the extent of known dioxin contamination Wi!~of the Roanoke River System above and below the discharge of the Weyerhaeuser l j!1, facility at Plymouth. Fish fillet analyses in 1990 evaluated 222 total individuals ~~/,! yielding 33 composites (Table 8). None of the locations sampled in 1990 above l(!i,~1.w __ illiamston, N.C. had average dioxin concentrations above 3 ppt expressed as a;;eiTEQ . Williamston, N.C. had been previously selected by the State Health .I~ Director as the upper bound for a dioxin fish consumption advisory on the f~~Roanoke River. In 1990, fish fillets in Welch Creek and the Roanoke River near ,~~-the Weyerhaeuser discharge continued to have elevated dioxin concentrations . . ,Jt•;ii):,, The maximum TEQ value observed in 1990 from the Roanoke system was found l~-;t:; in a composite sample of five channel catfish averaging 1409 grams in weight. s;':T-This maximum value was 26.4 ppt expressed as TEQ. In general, 1990 dioxin 11,~i information from the Roanoke system suggests lower fillet values when ;.g;';_ compared to data collected prior to 1990 (Table 9). Explanations for this change _..4,.,:;' would be consistent with the possibilities mentioned in the Neuse River. l'jJL: Samples collected from the Roanoke River at Weldon (Hatch) in 1988 were made ~7available for testing by staff of the Wildlife Resources Commission as a result of {f-J · fish hatchery activities on striped bass. The exact origin of these samples was not 11¥~• determined. ~I • ~J•:·" Table 8. Roanoke River System Dioxin Fish Fillet Summary For 1990 ?.~~r• ,,~-.;,·!l:1:-•{i.. Station Fish FiUet Sampled in 1990 li\11 ~(... Location Station Location Avg Num Num Num % obs ~(,;,-Number TE hi Obs S ecies ;, 3 TE ~~JY7 .-"'-"5"'2"""'-R-o_an_o_ke-Ri--v-er_a_t W-el_d_on_(_H_a_tc_h)-----'--"""---~!!!!..---"'>,a,._--"l.:="'------"--=--'"""~ I~,-._:;;:. ;! ~~:~~: ~:::~~:~~on ~:: !~ ~ : ~ ~£:..,. 1 55 Roanoke River at Williamston 0.2 37 4 3 O ,Jl,,. 56 (Roanoke River) Broad Cr. Slough lfJ7 5 5 7 8 Welch Creek at Highway 64 ~•·, Welch Creek Old Discharge Trowbridge Rd. -~-:Jh:. 59 Welsh Cr at old Weyerhauser discharge -·~Z "°. 60 Roanoke River near Weyerhauser discharge "· -··· 61 Middle River at NC 45 TI~'." 62 '1i!--;: 63 ii~ 64 '~~- 4'le;l"." 65 ~-1 66 l•~-r-;:~-67 ~~-tf.: ~--"'t,~ ;r;;~t r:.;,,.. .. . ,_ ) Albemarle Snd@ Terrapin Pt Roanoke River at Marker 15 Roanoke River at Sans Souci Roanoke River at Mouth Cashie River at Windsor Cashie River at Sans Souci F 0.4 0.4 38 31 19 25 222 total 7 5 4 4 33 total 5 4 4 2 100 40 0 0 20 average 14 0:: Figure 5. ROANOKE RIVER SYSTEM g; ii: :z: ;.;, }!,, ·.:: "!f ~> t th ) ~;;;...----,64 ·nJ,-=, "~,. i ;' .. ' •. ; ' ,· 0 3 APPROXIMATE SCALE (MILES) WEYERHAUSER i 0 :r: (.) ALBEMARLE SOUND@) t '1{ [) DIOXIN FISH MONITORING LOCATIONS □ MAJOR HIGHWAYS OTHER LOCATIONS SHOWN IN FIGURE 2 15 : I .~) . ; .. """·1 ,. • ,.. .~..1· . , ' ·• .. ~"'_··, ·7 .. . . - Current Fish Consumption Health Advisories for Dioxin in North Carolina Pigeon River No fish caught from the Pigeon River between Canton, N.C. and the Tennessee state line. should be consumed. Welch Creek Welch Creek --the entire creek Fish in Welch Creek may contain dioxins at levels of concern and should not be eaten. Swimming, boating, and other recreational activities present no health risks and are not affected by this advisory. Roanoke River Roanoke River --from to the mouth of the river emptying into Albemarle Sound. (Includes Broad Creek Slough) to the Highway 17 bridge near Williamston, N.C. Fish in the Roanoke River may contain low levels of dioxins. Consumption of fish should be limited to one meal per person per month. Children and pregnant or nursing women should not consume any fish from the Roanoke River until further notice. Swimming, boating, and other recreational activities present no health risks and are not affected by this advisory. Striped bass, herring, and shad (including roe) are not covered by this health advisory. Consumption of these three migratory fish species is not considered to present a health risk. Chowan River Chowan River --the entire length of .the river in North Carolina to the mouth emptying into Albemarle Sound. Catfish in the Chowan River may contain low levels of dioxins. Consumption of catfish should be limited to one meal per person every two months. Children and pregnant or nursing women should not consume any catfish from the Chowan River until further notice. All other fish in the Chowan River may be consumed with no ligiitations as they have not been found to contain significant dioxins. Swimming, boating, and other recreational activities present no health risks and are not covered by this advisory. Neuse River Neuse River --from Fort Barnwell to a line across the river from Johnson Point to McCotter Point (Minnesott Beach). Fish in this area of the Neuse River may contain low levels of dioxins. Consumption of fish should be limited to two meals per person per month. Children and pregnant or nursing women should not consume any fish from this area of the Neuse River until further notice. Striped bass, herring, and shad (including roe) are not covered by this health advisory. Consumption of these three migratory fish species is not considered to present a health risk. Note: These health advisories are only recommendations and do not constitute a regulatory ban on fishing or fish consumption. Advisories will be updated as necessary. 39 re·= JUTS To: File From: G.Doug Rumford~-~ Date: 6/26/95 Subject: Weyerhauser Co.-Plymouth Plymouth, Martin County, NC NCD 991 278 540 ••• ·11 REF. 34 Memorandum Wetlands, Critical Habitats, ·and Residential Population On this day, I reviewed the critical habitats inventory maps maintained by the NC Natural Heritage Program (NCNHP). One critical habitat was identified along the 15-mile site surface water pathway. The habitat of the Tidewater Muckel (Lampsilis ochracea), a freshwater mollusk classified by the State as being of Special Concern, is located in the Roanoke River approximately 6.5 miles downstream of PPE #2 -Former Weyerhauser discharge to Welch Cr. Huff Island has been identified as a breeding ground for the State dassified Significantly Ra~e Henslow's Sparrow (Ammodramus henslowii), and a habitat for the Significantly Rare Black Bear (Ursus americanus). The delta islands of the Roanoke River comprise the dedicated Federal Nature Preserve of the Tidal Cypress Gum Swamps. According to the topographic maps comprising the 4-mile site radius of the Weyerhauser facility, almost the entire area north of the site is a wetland. This area, approximately 8000 acres, was measured with a digital planimeter, the wetland acreage was not broken down per distance ring. The nearest wetland, relative to the former chlorine production building is a 40 acre island located in the Roanoke River 600 feet north. The total surface water pathway wetland frontage was measured to be approx. 13. 5 miles. A total of 50 residents have been identified by CGIA as living within 1 mile of the site although there were no households indicated within this distance. Visual observations of the area confirmed that no residences are present within 1 mile of the site. Consequently, the 50 residents indicated by CGIA have been disregarded as part of the population survey. Attachment. Ii • i II I IJ I I ' II 11 ,, '; I. '--• .! . . , .. ·, ' _, .. ; __ -+-· .,.._,._l ' --t- i '. I~: ,{,,'-l";:·,\ I. -, ~.- 2 LIST FORMAT species are grouped by major taxa. Th~ vertebrates-are arranged by class, beginning with the most advanced phyl~gem~t~cally (mammals). withi~ a givei;i ta1:'a, species are listed alphabetically by scientific name. The following inforrnat7on,is presented for each species on the list. "Status" is a word or phrase that 1.nd1.cates the degree of protection (if any), based on rarity, of a species; "rank" is a numerical scale of the rarity of a species, regardless of legal protection. Scientific Name. Common Name. For most groups, these names are not standardized. North Carolina Status. Endangered, Threatened, and special Concern species of Mammals, Birds, Reptiles, Amphibians, Freshwater Fishes, and Freshwater and. Terrestrial Mollusks have legal protection status in North Carolina (Wildlife Resources Commission). In addition to the above categories, the Natural Heritage Program maintains computer and map files on significantly Rare, Vulne~able, and Undetermined status species, as well as species considered Extirpated. Paper files only are maintained for some of the above species; these species are indicated by the phrase "not tracking." STATUS STATUS CODE E Endangered T Threatened SC Special Concern DEFINITION "Any native or once-native species of wlld animal whose continued existence as a viable component of the State's fauna is determined by the Wildlife Resources Commission to be in.jeopardy or any species of wild animal determined to be an 'endangered species' pursuant to the Endangered Species Act." (Article 25 of Chapter 113 of the General Statutes; 1987). "Any native or once-native species of wild animal which is likely to become an endangered species within the foreseeable future throughout all or a significant portion of its range, or one that is designated as a threatened species pursuant to the Endangered Species Act." (Article 25 of Chapter 113 of the General Statutes; 1987). · "Any species of wild animal native or once-native to North Carolina which is determined by the Wildlife Res6urcea Commission to require monitoring but which may be taken under regulations adopted under the provisions of this Article." (Article 25 of Chapter 113 of the General Statutes; 1987) • . SR EX w * # @ Significantly Rare Extirpated Watch List Any species which has not been listed by the N.C. Wildlife Resources Commission as an Endangered, Threatened, or Special Concern species, but which exists in the state in small numbers and has been determined by the N.c. Natural Heritage Program to need monitoring. (This is a N.C. Natural Heritage Program designation.) Significantly Rare species include "peripheral 11 species, whereby North Carolina lies at the periphery of the species' range (such as Purple Gallinule). The designation also includes marine and estuarine fishes identified as·"Vulnerable" by the N.C. State Museum of Biological Sciences (Roes et al., 1988, Endangered, Threatened, and Rare Fauna of North Carolina. Part II. A Re-evaluation of the Marine and Estuarine Fishes). Aleo included in the Significantly Rare designation are species formerly listed by the Natural Heritage Program (1991) as "Undetermined". "Undetermined" species are those that are secretive or are otherwise poorly known in North Carolina, which the Natural Heritage Program believes are rare and should be monitored. A species which is no longer believed to occur in the state. Any other species believed to be of conservation concern in the state because of scarcity, declining populations, threats to populations, ·or inadequacy of information to assess its rarity (see Page 33 for a more complete discussion). · Species is a game animal, and therefore (by law) cannot be liste~ for State protection as E, T, or sc. Species proposed for Endangered status, but not adopted by the Wildlife Resources Commission; species is protected from taking. species proposed for Special Concern status, but not adopted by the Wildlife Resources Commission; species is protected from taking. 3 il:· I ' I I j I I I i ,. ,. I i . ·~ -, ' ' I-= ,. ~-•-i I 1: .I Nehral Heritage Pr-ogr&11 List of the Rare Animls of lrlorth carol ina Scientific Name Province: Habitat Comnon Name Status Tadarida brasiliensis Brazilian Free-tailed Bat C: roosts in buildings and other man-made structures Trichechus manatus Uest Indian Manatee T: warm waters of estuaries and river mouths Ursus americanus Black Sear MC: extensive montane forests; pocosins, swan-ps BIRDS Accipiter cooperii Cooper's Hawk MPC: forests and woodlands (for nesting) [breeding evidence only] Accipiter gentilis Northern Goshawk M: extensive, remote forests, mainly et high elevations (for nesting) [breeding evidence only] Accipiter striatus Sherp·shiMed Hawk MP: forests end woodlands (for nesting) [breeding evidence only] Aegol ius acadicus Northern Saw·whet Owl M: spruce-fir forests or ·mixed hardwood/ spruce forests (for nesting) [breeding season only] Aimophila aestival is Bachmen's Sparrow CP: open longleaf pine forests, old fields [breeding season only] Arrmodrarus henslowii Henslow's Sparrow C: clearcut pocosins and other da111> weedy fields [breeding season only] Anhinga anhinga Anhinga. C: wooded talc.es or ponds, or open SWBIJl)S (for nesting) [breeding evidence only] Aquila chrysaetos Golden Eagle MC: extensive open country; formerly nested on cliffs [regular wintering O\ surmering sites] Bbtaurus lentiginosus American Bittern CT: fresh or braclcish marshes [breeding season only] CarrpeP.l'lilus principalis C: swarrps with mature tirrber Ivory-billed ~oodpeclcer [not traclcing; presl.lned extirpated in USA] Catharus guttatus Hermit Thrush M: spruce-fir forests (for nesting) [breeding season only] Charadrius melodus Piping Plover T: ocean beaches and island-end flats [breeding evidence only] Chordestes gralTJT18cus Lark. Sparrow C: barren, sandy fields with scattered saplings in the sandhills region [breeding season only] Circus cyaneus Northern Harrier T: extensive brackish marshes (for nesting) [breeding evidence only] Coccyzus erythropthalrus Blaclc-billed Cuclcoo M: deciduous forests, mainly et higher elevations [breeding season end habitat only] Colurbina passerine Corrmon Ground-Dove T: dunes, sandy fields, margins of maritime woods end thickets [breeding sea·s4?n only] Contopus boreal is Olive-sided Flycatcher M: montene conifer forests (mainly spruce-fir) with openings or deed trees [breeding season only] N.C. U.S. SC E SR* SC SR SR SC SC SR SR SR SR E SR T SR SR SR SR SC E C2 C2 C2 E T Rank N.C. Global SUB,S2N GS S1N G2? S3 GS S2B,S3N G4 SUB,SZN G4 S2B,S4N GS S2B,SZN GS S3B,S2N G3 S2B,S1N G4 S2B,SZN GS SXB7,S1N G4 S1B,S3N G4 sx G1 S1B,SSN GS S2B,S2N G3 S18,SZN GS S1B,S4N GS S2B,SZN GS S1B,S1N GS S1B,SZN GS 11 Scientific Name Province: Habitat llahral Heritage Prograa List of the Rare Aniaels of North Coomon Name Fusconaia masoni CP: most Atlantic drainages, end upper Coastal Plain; in lower Coastal Plain cariosa in lower Piednont also in Black River L~ilis PC: a nurber of Fall Line river systems; mainly near the L~ilis conspicuus P: Neuse, Flat, and upper Pee Dee riVers Larrpsilis crocata C: Lake Waccamaw and vicinity; possibly Orton Pond Larrpsilis fasciola M: French Broad, Pigeon, and Little Tennessee rivers; currently known only in last river Larrpsilis fullerkati C: Lake Waccamaw and vicinity (endemic to North Carolina and adjacent South Carolina) Larrpsilis ochracea CP: a nl.lrber of systems, primarily in the Coastal Plain; abundant in Lake ~accamaw Larrpsilis radiate CP: a nl.lrber of river systems Larrpsilis,·new species? (sp. 1) P: Deep River Lasmigona deCorata P: Catawba and Pee Dee drainages in Union and Mecklenburg counties (endemic to this.area and adjac·ent South Carolina) Lasmigona holstonia M: Watauga River; formerly in Valley Creek in Cherokee County Lasmigona subviridus CPH: Tar, Neuse, and Cape Fear systems downstate; New end Watauga systems in mountains Leptodea ochracea (see LelllJsilis) Ligunia nasuta C: Chowan, Roanoke, and Pamlico systems Pegias fabule M: Little Tennessee River; formerly in Valley 1· River in Cherokee County Strophitus undulatus P: Tar, Neuse, Cape Fear, and Pee Dee systems, perhaps other systems in Piecinont Toxolesma pullus PC: a nurber of Atlantic drainages, most nlJl'lerous in University Lake near Chapel Hill Tritogonia verrucosa M: New River near the Virginia border Villosa constricts PC: most Atlantic drainages, mainly in lower Piednont Villosa delurbis PC: most Atlantic drainages .Villosa nelx.!losa M: French Broad, Hiwassee, and Little Tennessee rivers; currently only known in the state from the last river Villosa vanuxemensis M: French Broad and Hiwassee Vil Losa vaughaniana P: Pee Dee system (endemic adjacent South Carolina) systems to North Carolina and Atlantic Pigtoe Yellow Lanprussel a bivalve Waccamaw Lanprussel Wavy-rayed LBllpll.lssel Waccamaw Fetll'l.lcket Tidewater Muck.et Eastern Lanprussel a bivalve Caroline Heelsplitter Tennessee Heelsplitter Green Floater Eastern Poncirussel Little-wing Pearlyrrussel Squewfoot Savannah Lilliput Pistolgrip Notched Rainbow Eastern Creek.shell Alabama Rainbow Mountain Creekshell Carolina Creek.shell carol ina Status N.C. U.S. T C2 T C2 SR SC SC T C2 SC SC SR E PE E C2 E C2 SC E E T T C2 E SR SR SC T SC N.C. Sl Sl SU S2 S2 Sl S2 S2 SU Sl , Sl Sl S2 Sl S2 S2 Sl S3? S3? S2 Sl S2 Rank Global G2 G4 G1G2Q G1Q (GU) G4 Gl G4 GS (G4) G1G2Q Gl G2 G4 (G3) G4 (G3) Gl GS (G4) G3 G4 G4 G3G4 G3 G4 G3 19 Mr. Steve Tedder, Chief Water Quality Section Department of Environment, Health, and Natural Resources Division of Environmental Management PO Box 27687 . Raleigh, North Carolina 27611-7687 Dear Mr. Tedder: re: Dioxin Analyses of Fish NPDES NO. NC0000680 PO Box 1391 New Bern, North Caro!iru. 28563·1391 ph. 919-633-7279 Fax 919-633-7634 Per the requirements of Weyerhaeuser Plymouth Mill's NP DES permit, enclosed is a report covering fish dioxin studies during the fall of 1993. Two copies of the report are provided. These studies were conducted with fish from the Roanoke River, Chowan River, and Albemarle Sound. Please call if you have any questions about aspects of the study not covered in the report (919-633-7351). Sincerely, ~,l._._ c c.Y~J_ Stephen E. Woock Aquatic Scientist -Weyerhaeuser cc : John Pritchard, Plymouth Mill -iA IJ·~ Weyerhaeuser RESEARCH REPORT SOUTHERN ENVIRONMENTAL FIELD STATION ES&T Research & Development New Bern, NC 28563 lJ Technical Report □ Technical Note □ Trip Report □ Other Title Page Project No. 044-9309 Page I of39 ROANOKE RIVER, CHOWAN RIVER/HWY17, AND ALBEMARLE SOUND FISH DIOXIN NPDES STUDY PROJECT NO. 044-9309 September -November 1 993 ********* Prepared for Weyerhaeuser Pulp and Paper Mill Plymouth, North Carolina for submittal to NCDEM ********* Strictly Proprietary (Red): Disclosure strictly limited to persons on a managed list. Contact David McHenry Proprietary (Yellow): Disclosure limited to persons confidentially bound to Weyerhaeuser on a need to know basis. Non-Proprietary (Green): Disclosure unlimited .. PLY/94/93PFISDX.DOC 3/16194 f:l!X3if6VCletll\'WRtt:'.Z rrnrrr tr:rnr \. R .. ·' ,U:-,-j';:,· I ~ '~:: ', 1:: 'II ,I 11 ' 11 11 ' I j, . ., ,--- -~---' i~--1:~, 1:· -· ,:_ ,,- 1 A RESEARCH REPORT ES& T Southern Environmental Field Station Research & Development Executive Summary Project No. 044-9309 Page 2 of39 Fish fillets from the Roanoke River upstream and downstream of the Plymouth Mill, the mouth of the Chowan River at Albemarle Sound, and western Albemarle Sound were analyzed for tetrachlorinated dioxins and furans. The sampling was conducted to fulfill an NPDES requirement from the North Carolina Division of Environmental Management (NCDEM) and to monitor time trend changes in fish dioxin concentrations. The fish were col.lected during September through November of 1993. The report provides transfer of the dioxin data and ancillary information to NCDEM. Dioxin toxicity equivalent (TEO) is a measure of the summed concentrations of the chlorinated dioxin and furan congeners, each expressed as the potential toxicity of 2,3,7,8-TCDD. In this study, only the 2,3,7,8-and total-tetrachlorinated dioxin and furan congeners were measured; thus the TEOs are based only on the concentrations of 2,3,7,8-TCDD and 2,3,7,8 -TCDF. For all species, individual fillet sample concentrations of 2,3,7,8-TCDD ranged from non-detect to 18.5 ppt. The TEOs ranged from 0.03 to 4.5 parts per trillion (ppt) among all the sampled fish species except channel catfish. D.ioxin (TEO) concentrations in channel catfish fillets were usually greater than the other species at each location; channel catfish TEOs ranged from 0.81 ppt upstream at Williamston, to 19.55 ppt downstream at Highway 32 in Albemarle Sound. Channel catfish have greater dioxin concentrations because they have greater lipid 1 content compared with the other fish species sampled. The greater lipid pool in the channel catfish provides a storage site for dioxins due to the tendency for dioxin to partition strongly into lipids. Comparing years, reported average TEO for the river and sound stations was one ppt less in 1993 than in 1992. Excluding the upstream station at Williamston, average TEO was 3.6 ppt in 1993 versus 4.6 ppt in 1992. However, for most of the individual stations and fish species the lower 1993 concentrations can be explained by decreases in average weight or lipid content of captured fish, particularly catfish. In contrast, gamefish concentrations of 2,3, 7,8-TCDD were similar to 1992 with slight increases noted among Albemarle Sound striped bass samples. It is important to note that the general lower average weights of fish captured in 1993 were not due to changes in sampling techniques or gear but rather to inherent variability of fish sizes encountered during annual collecting periods. Strictly Proprietary (Red): Disclosure strictly limited to persons on a managed list. Contact Proprietary (Yellow): Disclosure limited to persons confidentially bound to Weyerhaeuser on a need to know basis. Non-Proprietary {Green): Disclosure unlimited. PLY/94/93PFISDX.DOC 3/16/94 I I I I I I I I I I I I I I I I I MEMORANDUM TO: File FROM: G.Doug Rumford Hydrogeologist, DATE: 10/11/96 REF. 36 NC Superfund SUBJECT: Georgia-Pacific Corp. Hardwood Sawmill Plymouth, Washington County, NC NCD 000 813 592 Ownership of Adjacent Property On this day I spoke with Lynn at the Washington County Register of Deeds in Plymouth, NC to inquire about the property located near the gate to the former hardwood sawmill, adjacent to Plymouth High School. This property (Parcel 2545, Block 99, Map 6767.08) is currently owned by the Boy Scouts of America; the deed was tranferred on February 11, 1948 from the seller, Still Realty. I I I I I I I I I I I I I I I I I I I MEMORANDUM TO: File FROM: G.Doug Rumfor~ Hydrogeologist, Jll: Su~rfmd DATE: 6/2/95 REF. 37 SUBJECT: Georgia-Pacific Corp. Hardwood Sawmill Plymouth, Washington County, NC NCO 000 813 592 Telecon with Mike Beachum, Outerbanks Contractors On this day I spoke with Mike Beachum ofOuterbanks Contractors (919-261-2255) regarding the former Georgia-Pacific Hardwood Sawmill plant in Plymouth, NC. Mr. Beachum told me that Outerbanks Contractors leased the property from Decatur Partnerships. Outerbanks Contractors, a subsidiary of Decatur Partnerships, used the southern portion of the property for an asphalt mixing facility. The site is not currently in use by either Outerbanks Contractors or Decatur Partnerships. I told Mr. Beachum that on June 19, 1995, a site visit was planned and that sampling would be conducted during the trip. He gave me access authorization to sample on the site and mentioned that he was not interested in collecting any split samples. I ·.~ I ' I ' ' ___ :,. I I I I 1· I I , .. ,·-. 'ii'/ ,,, ' u ,I I I I I I I -1,, , REF. 38 SUPERFUND CHEMICAL DATA MATRIX APPENDIX B TABLES :1;. I~. ·•.•o.J I I .I ·I I 1· I l·:t ,..:,..• I I 0 I u I I \:t•· I ,, Appendix B-1 Tables for Non-Radioactive Hazardous Substances I I I I I I I I I I I I- I I I I I I 1- REF. 39 Inactive Hazardous Sites Program Guidelines for Responsible Party Voluntary Site Remedial Action October 1996 North Carolina Department of Environment, Health and Natural Resources Division of Waste Management Superfund Section Inactive Hazardous Sites Branch Post Office Box 27687 Raleigh, North Carolina 27611-7687 Telephone: (919) 733-2801 I I I I I I I I I I -• I I I I I I Attachment C: Inactive Hazardous Sites Branch Health Based Remediation Goals for Soil and Groundwater Table C-1: Soil Remediation Goals (RG's) * Cleanup below method detection limits, using analytical methods prescribed in these guidelines, is not required This list is not meant to be comprehensive. The Branch will calculate RG 'sf or chemicals not listed on the table if a request is submitted in writing. 21z § • ~i•i')f!;fi)V) :,•,:. Acetone 67641 Acetone cyanohydrin 75865 Acetonitrile 75078 Acetoohenone 98862 Acrolein 107028 Acrylamide 79061 Acrvlic acid 79107 Acrylonitrile 107131 Aldicarb I 16063 Aldrin 309002 Allvl alcohol 107186 Allvl chloride 107051 4-Aminonvridine 504245 Ammonium sulfarnate 7773060 Aniline 62533 Antimony and comoounds 7440360 Antimony oentoxide 1314609 AntimonY ootassium tartrate 304610 Antimony tetroxide 1332316 Antimony trioxide 1309644 Arsenic 7440382 Benzene 71432 Benzenethiol 108985 Benzidine 92875 Benzoic acid 65850 Benzotrichloride 98077 Adapted from USEPA Regjon Ill Risk. Based Concentration Table, except as noted. The RG is based on the carcinogenic endpoint and corresponds to an excess lifetime cancer risk of I in 1,000,000. The RO is based on USEPA guidance on lead cleanup levels. ,. 2:.1 , 1560 N I 100 N 94 N 1560 N 320 N 0.14 C 7800 N 1.2 C 15.6 N 0.038 C 78 N 780 ;-,;N 0.32 N 3200 N 110 C 6.2 N 7.8 N 14 N 6.2 N 6.2 N 4.6 N 22 C 0.156 N 0.0028 C 62000 N 0.049 C • C L N The RO is based on the non-carcinogenic endpoint and ~esponds to a hazard quotient of0.2. Final RG a tabulated RO x 'I.~ where n .. number of non-carcinogens and docs not exceed 5. NA - p Not Available. The RO ~ based on USEP A PCB sp;JJ policy. Table C-1: Soil Remediation Goals (RG's)* -(Cont.) w ~-CA<ITiNY /f::, :-.::-; i R/i iiiiihil ··•·• •· .,., " < ··•··.· "-~·I chloride 100447 Rervlliwn and comnnunds 7440417 alnhaBHC 319846 l. betaBHC 319857 oarnma BHC n indane) 58899 technical BHC lhexachlorn=clohexane, all isomers) 608731 Bisf2-chloroethvl\ether I I I 444 Bisf2-ethvlhexv})nhthalate ffiEHP) 117817 Bis! chloromethvl.-ther 542881 Bromodichloromethane 75274 Bromoform (tribromomethane) 75252 Bromomethane 74839 4-Bromoohenvl ohenvl ether 101553 1-Butanol 71363 Butvl ben7V} ohthalate 85687 CacNivlic acid 75605 Cadmium and comoounds 7440439 Cantan 133062 Carharvl 63252 Carbon disulfide 75150 Carbon tetrachloride 56235 Chloral 75876 Chlordane 57749 Chlorine 7782505 2-Chloro-1,3-butadiene 126998 4-Chloro-2,2-methvlaniline hydrochloride 3165933 4-Chloro-2-methvlaniline 95692 . Chloroacetaldehvde 107200 * ·c 4-Chloroaniline 106478 Chlorobenzene 108907 Chlorobenzilate 510156 4-Chlorobenzotrifluoride 98566 1-Chlorobutane 109693 Adapted from USEPA Region III Risk Based Concentration Table, except as noted. The RG is based on the carcinogenic endpoint and corresponds to an excess lifetime cancer risk of I in 1,000,000. The RG is based on USEPA guidance on lead cleanup levels. 3.8 0.15 0.1 0.35 0.49 0.35 0.58 46 0.0029 JO 81 22 900 1560 3200 46 7.8 180 1560 1560 4.9 32 0.49 1560 320 1.4 I.I 108 62 320 2.4 320 6200 C C C C C C C C C C C N N N N N N C N N C N C N N C C N N N C N N L N The RO is based on the non-carcinogenic endpoint and corresponds to a hazard quotient of0.2. Final RO• tabulated RO x 'I.; where n = number of non-carcinogens and docs not exceed 5. NA · p Not Available. The RG is based on USEPA PCB spill policy. C-2 I I I I I I I, I ,, I"" 1· I:: I I I I I I I I I I I I I I I I I I I I I I I I I I Table C-1: Soil Remediation Goals (RG's)* -(Cont.) :.::,::((/·:::::::;:::::\/11 ... , F•••.>••·•Xt'Che~iJ111•• i::f//f:; ;·, ····.;.;,, ... , <•••·?+•T:/1 ?cA:i;;kN.'iltl t•i<••·•••·tRGi :..:.';;;; //./::?i:\'=:: :;,:··.:,:.:_',.;-,::.:=::::t:::: Cblorodibromomethane 124481 Chloroethane 75003 2-Cbloroethvl vinvl ether I 10758 Chloroform 67663 Cbloromethane 74873 beta-Cbloronaphthalene 91587 o-Cbloronitrobenzene 88733 p-Cbloronitrobenzeae !00005 2-Cbloropheno! 95578 o-Cblorotoluene 95498, Chlomvrifos 29213~2 Chror.1ium III and comoounds 160638:, 1 Chromium VI and comoounds 1S5<0299 Coooer and compounds 7440508 Crotonaldehvde 123739 Cumene 98828 r,,anhle.~.· I I Barium cvanide 542621 Calcium cyanide 592018 Copper cvanide 544923 Cvnnazinc 2 I 725452 Cvanm!en 460195 Cvanoe:e:1 bromide 506683 Cvaooien chloride 506774 Free cyanide 57125 Hvdrogcn cvaoide 74908 Potassium cvanide 15150~ - P0tassium silver cvanide I 5066 ](, Silver cyanide 5066.J9 Sodium cvanide 143339 Thiocvaoate NA Zinc cvanide 557211 Cvclohexanone 108941 Adapted from USEPA Region III Risk Based Concentration Table, except as noted. The RO is based on the carcinogenic endpoint and corresponds to Dn excess lifelime cancer risk of I in 1,000,000. The RO is based on USEPAguidance on lead cleanup levels. 7.'6 C 6200 N 400 N !CO C 49 C 1260 N 26 C 35 C -7S N 320' N 46 N 156!JD1 .N 73! is/ 620 N 0.34 C 620 N I 1560 N 620: N 78 N 0.76 C 620 N 1400 N 780 N 320 N 320 N ---/ ,),J' N 3:00 N ' l56C: N 6201 N ' 32lli N 7RO N 780001 N ... • C L N The RO is based on the non-carcinogenic endpoint and corresponds to a hazard quotient of0.2. Final RG .. tabulated RG x 'I.; wht..-re n ... number of non-carcinogens and does not exceed 5. · NA -p Not Available. The RO ~ based on USEPA PCB sp;u pohcy. C-3 Table C-1: Soil Remediation Goals (RG's)* -(Cont.) ~ 0 .. 0: t:A/,;RN/• ···•·<•·••·····/·••J?(J.•1;;;;;;.~ 2-r.vclohexvl-4,6-dinitroohenol ( 4,6-Dinitro-o-cvclohexvl ohenol) 131895 Dalanon 75990 DDD 72548 DDE 72559 DDT 50293 Diallate 2303164 Diazinon 333415 Dibenzofuran 132649 l ,2-Dibromo-3-chloropropane 96128 1,2-Dibromoethane 106934 Di-n-butvl phthalate 84742 Dicamba 1918009 1,2-Dichlorobenzene 95501 1,3-Dichlorobenzene 541731 1,4-Dichlorobenzene 106467 3,3'-Dichlorobenzidine 91941 Dichlorodifluoromethane 75718 - * C L 1, 1 :bichloroethane 75343 1,2-Dichloroethane ll'DC) 107062 1, 1-Dichloroethvlene 75354 1,2-Dichloroethvlene ( cis) 156592 1,2-Dichloroethvlene (mixture) 540590 1,2-Dichloroethvlene (transl 156605 2,4-Dichloroohenol 120832 2,4-Dichlorophenoxvacetic acid (2,4-Dl 94757 1,2-Dichloropropane 78875 2,3-Dichloroorooanol 616239 1,3-Dichloropropene 542756 Dichlorvos 62737 Dicofol 115322 Dieldrin 60571 Diethvl ohthalate 84662 Diethvlstilbestrol 56531 Adapted from USEPA Region III Risk Based Concentration Table. except as noted. The RG is based on the carcinogenic endpoint and corresponds to an excess lifetime cancer risk of 1 in 1,000,000. The RG is based on USEPA guidance on lead cleanup levels. 32 N 460 N 2.7 C 1.9 C 1.9 C 10 C 14 N 62 N 0.46 C 0.0075 C 1560 N 460 N 1400 N 1400 N 27 C 1.4 C 3200 N 1560 N 7 C I.I C 156 N 140 N 320 N 46 N 156 N 9.4 C 46 N 3.7 C 2.2 C 1.5 C 0.04 C 12600 N 0.00014 C N The RO is based on the non-carcinogenic endpoint and corresponds to a hazard quotient of0.2. Final RG ""tabulated RG x 5/~ where n"' number of non-carcinogens and does not exceed 5. NA. p Not Available. The RG is based on USEPA PCB spill policy. C-4 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I Table C-1: Soil Remediation Goals (RG's)* -(Cont.) ~ •••••·••·CA:Cffi.NL /ti: <\••F{[{G ',"" -· Dimethoate 60515 3.2 N; 3.3'-Dimetho=benzidine 119904 46 C 3,3'-Dimethvlbenzidine 119937 0.069 C 1, 1-Dimethvlhvdrazine 57147 0.25 C 1.2-Dimethvlhvdrazine 540738 0.017 C 2,4-Dimethvlohenol 105679 320 N Dimethvl ohthalate 131113 156000 N 1,2-Dinitrohenzene (o-Dinitrohenzene) 528290 6.2 N 1,3-Dinitrobenzene (m-Dinitrobenzene) 99650 1.56 N 1,4-Dinitrobenzene fn-Dinitrobenzene) 100254 6.2 N 2.4-Dinitronhenol 51285 32 N 2,4-Dinitrotoluene 121142 32 N 2,6-Dinitrotoluene 606202 15.6 N Dinitrotoluene mixture NA 0.94 C Dinoseb 88857 15.6 N 1,4-Dioxane (o-Dioxane) 12391 I 58 C -· ,.._,1 ~ 2,3,7 ,8-H~tachlorodibenzo-o-dioxin (2,3,7 ,8-HPeCDDl NA 0.0004 c· 2,3, 7 ,8-Hexachlorodibenzo-o-dioxin (2,3, 7 ,8-HxCDD) NA 0.00004 ,, c· .. Octachlorodibenzo-n-dioxin (OCDD) NA 0.004 C 2,3,7 ,8-Pentachlorodibenzo-n-dioxin (2,3,7 ,8-PeCDD) NA 0.000008 C 2,3,7 ,8-Tetrachlorodibenzo-n-dioxin (2,3,7 ,8-TCDD) 1746016 0.000004 C 2,3, 7 ,8-Hentachlorodibenzofuran 12,3, 7 ,8-HPCDFl NA 0.0004 C 2,3, 7 ,8-Hexachlorodibenzofuran 12,3,7 ,8-HxCDF) NA 0.00004 C Octochlorodibenzofuran (OCDF) NA 0.004 C 1,2,3, 7 .8-Pentachlorodibenzofuran /J ,2,3,7 ,8-PeCDF) NA 0.00008 C 2,3,7 ,8-Pentachlorodibenzofuran /2,3,7 ,8-PeCDF) NA 0.000008 C , 1 7 R-Tetrachiorodiben,ofura" '2 l 7 8-TrDF\ NA . 0(10004 C Diohenvlamine 122394 400 N 1,2-Diohenvlhvdrazine 122667 0.8 C Diauat 85007 34 N Disulfoton 298044 . 0.62 N Diuron 330541 32 N Adapted from USEPA Region III Risk Based Concentration Table, except as noted. • C L N The RG is based on the c:arcinogenic endpoint and corresponds to an e~ lifetime cancer risk of I in 1,000,000. The RG is based on USEPA guidance on lead cleanup levels. The RG is based on the non-carcinogenic endpoint and corresponds to a hazard quotient of0.2. Final RO= tabulated RG x 't.;. where n .. number of non-carcinogens and docs not exceed 5. NA - p Not Available. The RO is based on USEPA PCB spill policy. C - 5 Table C-1: Soil Remediation Goals (RG's)* -(Con£) ~ ~ VCA!{kN.r : ,r:r:•·•'••k{;1,;,;,;;1_J Endosulfan I I 5297 Endothall 145733 Endrin 72208 Eoichlorohvdrin 106898 Ethion 563122 2-Etho=ethanol I 10805 Ethv I acetate 141786 Ethv I •=late 140885 Ethv !benzene 100414 Ethvlene diamine 107153 Ethvlene oxide 75218 Ethvlenethiourea i'ETU) 96457 Ethvl ether 60297 Ethvl methacrvlate '97632 Fonnaldehvde 50000 Fannie acid 64186 Furan 110009 Furfural ~-98011 Glvcidaldehvde 765344 Hentachlor 76448 Hentachlor enoxide 1024573 Hexachlorobenzene 118741 Hexachlorobutadiene 87683 Hexachlorocvclopentadiene 77474 Hexachloroethane 67721 Hexachloroohene 70304 · Hvdrazine 302012 Hvdrooen sulfide 7783064 Isoohorone 78591 K~ne 143500 Lead 7439921 Malathion 121755 Maleic anhvdride 108316 Adapted from USEPA Region III Risk Based Concentration Table, except as noted. The RO is based on the carcinogenic endpoint and corresponds to an excess lifetime cancer risk of I in 1,000,000. The RO is based on USEPA guidance on lead cleanup levels. 94 320 4.6 65 7.8 6200 14000 13 1560 320 0.63 5.4 3200 1400 3200 32000 15.6 46 6.2 0.14 0.07 0.4 8.2 110 46 4.6 0.21 46 670 0.035 400 320 1560 }},') N N N C N N N C N N C C N N N N N N N C C C C N C N C N C C L N N • C L N The RG is based on the non~ogenic endpoint and corresponds to a hazard quotient of0.2. Final RG = tabulated RG x 'I.; where n = number of non~gcns and does not exceed 5. NA • p Not Available. The RG is based on USEPA PCB spill policy. C-6 I I I I I I I 1·· I I I I I I I I I I --I II I Ii I I ' II I I I II I Ill I I I * C L Table C-1: Soil Remediation Goals (RG's)* -(Cont.) , .... ~·c• •·· /ii.·••···· •••··.· ri,emical ··•·· . · .. >.: I CASRN :••·I <i .: <·•RG.inrinil• Maleic hydrazide 123331 Malononitrile 109773 Merclll1' (inon:anic) 7439976 Methacrvlonitrile 126987 Methanol 67561 Methomvl 16752775 Metho""chlor 72435 2-Methvl benzenamine (2-methvlaniline) 95534 2-Methvl benzenamine hvdrochloride (2-methvlaniline hvdrochloride' 636215 Methvl chlorocarbonate 79221 4,4'-Methylene bis(2 chloroaniline) 101144 Methylene bromide 74953 Methylene chloride 75092 Methyl ethyl ketone IMFK) 78933 Methvl hydrazine 60344 Methyl isobutvl ketone (4-methvl-2-pentanone) 108101 Methvl methacrvlate 80626 Methvl parathion 298000 3-MethvlPhenol (m-cresol) 108394 2-Methvlohenol ( o-cresoll 95487 4-Methylphenol io-cresol) 106445 2-Methly -1-propanol (isobutanol, isobutvl alcohol) 78831 Naled 300765 2-Naohthvlamine 91598 Nickel and comoounds 7440020 Nitric oxide 10102439 4,Nitroaniline 100016 Nitrobenzene 98953 Nitrogen dioxide 10102440 4-Nitroohenol 100027 2-Nitropropane 79469 N-Nitrosodiethanolarnine 1116547 N-Nitrosodiethvlamine 55185 .. Adapted from USEPA Region Ill Risk Based Concentration Table, except as noted. The RO is b4sed on the carcinogenic endpoint and corresponds to an excess lifetime canctr risk of 1 in 1,000,000. The RO is based on USEPA guidance on lead cleanup levels. 7800 0.32 4.6 1.56 7800 400 78 2.7 3.5 15600 4.9 156 85 9400 0.58 1260 1260 4 . 780 - 780 78 4600 32 0.0049 320 1560 46 7.8 15600 960 0 0.23 0.0043 ····•:·•·•:•::\·: N ·N ·N N N N N C C N C N C N C N N N N N N N N C N N N N N N N C C N The RO is based on the non-carcinogenic endpoint and corresponds to a hazard quotient of0.2. Final RG = tabulated RG x 'I.~ where n = nwnber of norH:areinogcns and does not exceed 5. NA· p Not Avai1ab1e. The RG i, based on USEPA PCB spill policy. C-7 .. Table C-1: Soil Remediation Goals (RG's)* -(Cont.) .\ .............. <•·• i ; < >Chemical \ r C -··•.• \ ··•· . . CAf.JRN .· ·· kGf;,;,"ii,l > >·•· N-Nitrosodirnethvlamine 62759 0.013 C N-Nitrosodi-n-butvlamine 924163 0.12 C ' N-Nitroso di-n-pronvlamine 621647 0.091 C N-Nitrosodiohenvlamine 86306 130 C N-Nitroso-N-ethvlurea ( ethvlnitrosourea) 759739 0.0046 C N-Nitrosonvnnlidine 930552 0.3 C o-Nitrotoluene 88722 156 N m-Nitrotoluene 99081 156 N o-Nitrotoluene 99990 156 N Octamethvlnvrnnhosnhoramide 152169 32 N di-n-Octvl ohthalate 117840 320 N Paraauat 1910425 70 N Parathion 56382 94 N Pentachlorobenzene 608935 12.6 N Pentachloronitrobenzene 82688 2.5 · C Pentachloroohenol 87865 5.3 C Phenol 108952 9400 N p-Ph'envlenediamine 106503 3000 N Phenvlmercuric acetate 62384 1.26 N Phorate 298022 3.2 N Phosnhine 7803512 4.6 N Phosnhorus (white) 7723140 0.32 N Phthalic anhvdride 85449 32000 N Polychlorinated biohenyls (PCBs) 1336363 I p -. Acenaohthene 83329 940 N Anthracene 120127 4600 N Bonzo[ a lnvrene 50328 0.088 C Benzofb lfluoranthene 205992 0.88 C Benzofk lfluoranthene 207089 8.8 C Benzr al anthracene 56553 0.88 C Carbofuran 1563662 78 N Chrvsene 218019 88 C • Adapted from USEPA Region llI Risk Based Concentration Table, except as noted. C L N The RG is based on the carcinogenic endpoint and con-esponds to an excess lifetime cancer risk of 1 in 1,000,000. The RG is based on USEPA guidance on lead cleanup levels. The RG is based on the non-carcinogenic endpoint and corresponds to a hazard quotient of0.2. Final RG = tabulated RG x 'I.; where n"" number of non-carcinogens and docs not exceed S. NA. p Not Available. The RG is based on USEPA PCB spill policy. C-8 I I I I I I II II II II I II I I I I I -1 I I I I I I I I I I I I Table C-1: Soil Remediation Goals (RG's)* -(Cont.) I ,, 2 ~ ·~'·'· ii: ' C:4.SRN( ·:.::.;: :-:.\ >k(;i, :C::":C: Dibenzf ah lanlhracene 53703 0.088 C Fluoranthene 206440 620 N Fluorene 86737 620 N Indennfl ,2,3-cd\nvrene 193395 0.88 C N aohthalene 91203 620 N o.~e 129000 460 N Pronamide 23950585 1180 N Prooaroite 2312358 320 N Proparovl alcohol 107197 32 N Pmnazine 139402 320 N Pronvlene oxide 75569 2.7 C Pvridine 110861 15.6 N Quinoline 91225 0.053 C Selenious acid 7783008 78 N Selenium 7782492 78 N Selenciurea 630104 78 N Silver and comoounds 7440224 78 N Sodium azide 26628228 62 N - Sodium fluoroacetate 62748 0.32 N Strvchnine -57249 4.6 N Stvrene 100425 .. 3200 N 2,3,7,8-TCDD /dioxin\ 1746016 ---4. !0e-06 C 1,2,4,5-Tetrachlorobenzene 95943 4.6 N I, 1,2,2-Tetrachloroethane 79345 3.2 C I, I, 1,2-Tetrachloroethane 630206 25 C Telrachloroethvlene /PCE) 127184 12 C 2,3,4,6-Tetrachloronhenol 58902 460 N p,a,a,a-Tetrachlorotoluene 5216251 0.032 C Tetraethvldithionvmnhosnhale 3689245 7.8 N Tetraethvl lead 78002 0.00156 N Thallic oxide 1314325 1.1 N Thallium NA 1.26 N Thallium acetate 563688 1.4 N Adapted from USEPA Region m Risk Based Concentration Table, except as noted. * C L N The RG is based on the carcinogenic endpoint and corresponds to an excess lifetime cancer risk of I in 1,000,000. 1be RG is based on USEPA guidance on lead cleanup levels. The RO is based on the non~ogenic endpoint and corresponds to a hazard quotient of0.2. Final RO• tabulated RO x 'I.; where n .. number ofnotKarcinogens and does not exceed,. NA - p Not Available. The RO is based on USEPA PCB spill 1X>licy. C-9 Table C-1: Soil Remediation Goals {RG's)* -(Cont.) ,',, ' ·~ '\ >CASRNT •:;,c:,·;;,:,:>,)?GiliiiliJ.,. ., ·~ Thallium carbonate 6533739 1.26 N Thallium chloride 7791120 1.26 N Thallium nitrate 10102451 1.4 N Thallium selenite 12039520 1.4 N Thallium sulfate 7446186 1.26 N Thiofanox 39196184 4.6 N Thiram 137268 78 N Toluene !08883 3200 N Toluene-2,4-diamine 95807 0.2 C Toluene-2,6-diamine 823405 3200 N o-Toluidine 106490 3.4 C Toxaohene 8001352 0.58 C I, 1,2-Trichloro-1,2,2-trifluoroethane 76131 200000 N 1,2,4-Trichlorobenzene 120821 156 N I, I, I-Trichloroethane 71556 540 N I , 1,2-Trichloroethane 79005 11 C Trichloroethylene (TCE) 79016 58 C Tricnlorofluoromethane 75694 4600 N 2,4,6-Trichlorophenol 88062 58 C 2,4 ,5-Trichlorophenol 95954 1560 N 2-(2,4,5-Trichlorophenoxv)oropionic acid 93721 126 N 2,4,5-Trichlorophenoxvacetic acid 93765 156 N I, 1,2-Trichloroorooane 598776 78 N 1,2,3-Trichloroorooane 96184 0.091 C 1,3,5-Trinitrobenzene 99354 0.78 N Vanadium nentoxide 1314621 140 N Vinyl acetate 108054 15600 N Vinyl chloride 75014 0.34 C o-Xvlene 95476 32000 N m-Xvlene 108323 32000 N Xvlene /mixed) 1330207 32000 N Zinc 7440666 4600 N Zinc phosphide 1314847 4.6 N Adapted from US EPA Region III Risk Based Concentration Table, except as noted. * C L N 1bc RG is based on the carcinogenic endpoint and correspond., to an excess lifetime cancer risk of I in 1,000,000. 1be RG is based on USEPA guidance on lead cleanup levels. The RO is based on the non-carcinogenic endpoint.and corresponds to a hazard quotient of0.2. Final RG '"'tabulated RG x 'I.; where n • number of non-carcinogens and does not exceed S. NA -p Not Available. The RG is based on USEPA PCB spill policy. C -IO I I I I I I I I I- I_ I I I I I I I I I I I I I I I I I I I I I I I I I Table C-2: Groundwater Remediation Goals (RG's)1.2 Cleanup be/aw method detection limits, using analytical methods prescribed in these guidelines, is not required This list is not meant to be comprehensive. The Branch will calculate RG 's for chemicals not listed on the table if a request is submitted in writing. ~ ~'<'D1'L~ \(ii?/i/RG.••@fab)•' f i.:::::C:: ,- Acenaphthene 83329 80 Acenaphthylene 208968 210 Acetone 67641 700 Acrylamide 79061 0.01 Aldicarb' 116063 7 Ammonia' 7664417 1100 Anthracene 120127 2100 Antimony' 7440360 6 Arsenic' 7440382 0.045 Barium 7440393 2000 Benzene 71432 I Benzo(a)anthracene 56553 0.0479 Beryllium 7440417 -4 Bis(2-ethylhexyl)phthalate 117817 .. 3 , .. Bromodichloromethane 75274 0.56 Bromofonn 75252 0.19 Butyl benzyl phthalate 85687 100 Cadmium 7440439 5 Caprolactarn 105602 3500 Carbon disulfide 75150 700 Carbofuran 1563662 36 Carbon tetrachloride 56235 0.3 Chlordane 57749 0.027 I Chlorobenzene 108907 50 Chlorodibromomethane' 124481 80 Chloroform 67663 0.19 2-Chlorophenol 95578' 0.1 Chromium 744073 50 Chrysene 218019 4.79 Copper 7440508 1000 See footnotes at the end of Table C-2. C -11 'I I --. ,I • .• ' lo, Table C-2: Groundwater Remediation Goals (Cont.) ~ ~ r•51'i;,11N\··,.,.,.···•·'> } }{RG.'.'(ftpb) {r'···•,·,.,·,, ...... Cyanide 57125 154 1.2-Dibromo-3-<:hloropropane 96128 0.025 1,2-Dicblorobenzene 95501 620 1,3-Dicblorobenzene 541731 620 1,4-Dichlorobenzene 106467 75 Dichlorodifluoromethane (Freon-12) 75718 1400 1,1-Dichloroethane 75343 700 1,2-Dichloroethane 107062 0.38 I, 1-Dichloroethylene 75354 7 cis-1,2-Dichloroethylene 156902 70 trans-1,2-Dicbloroethylene 156605 70 2,4-Dichlorophenoxy-acetic-acid (2,4-D) 94757 70 1,2-Dichloropropane 78875 0.56 1,3-Dichloropropene 542756 0.19 Diethyl p!Jthalate 84662 5000 Di-n-butyl phthalate 84742 700 Diquat• 85007 20 para-Dioxan~ 12391 I 7 Dioxin 1746016 2.2 X 10"7 Endosulfan 7 I 15297 42 Endrin 72208 2 Ethlylbenzene 100414 29 Ethylene dibromide 106934 0.0004 Fluoranthene 206440 280 Formaldehyde' 50000 1400 Heptacblor 76448 0.008 Heptacblor epoxide 1024573 0.004 Hexachlorobenzene I 18741 0.02 Hexachlorobutadiene• 87683 I ' Hexachlorocyclopentadiene' 608731 50 Lead 7439921 15 Lindane 58899 0.2 Mercury 7439976 1.1 See footnotes at the end of Table C-2. C-12 . - I I I I I I I I I I I I I I I Ill I I I Table C-2: Groundwater Remediation Goals (Cont.) I -• I I I I I I I I I •··•·· .... ~ Methanol Methoxychlor Methyl ethyl ketone 4-Methyl phenol' Methylene chloride Napthalene Nickel Pentachlorophenol Phenol PCB's' Pyrene Selenium Silver Styrene 2,4,5-TP' 1,2,4,5-Tetrachlorobenzene' I, 1,2,2-Tetrachloroethane' Tetrachloroethylene Thallium' Toluene Toxaphene 1,2,4-Trichlorobenzene' I, I, I-Trichloroethane I, 1,2-Trichloroethane• Trichloroethylene Trichlorofluoromethane Vinyl chloride Xylenes Zinc I Footnotes listed on the following page. I -~' I C-13 I Xii )( >·•·•··· ?RG•'(ppb)t·••• r·•·rr·•·•··· · 67561 ' 3500 72435 35 78933 170 106445 35 75092 5 91203 21 7440020 100 87865 0.3 108952 300 1336363 0.5 129000 210 7782492 50 7440224 18 100425 100 93765 50 95943 . 2• I 79345 0.167 127184 0.7 7440280 0.5 108883 1000 8001352 0.031 120821 70 71556 200 79005 3 79016 2.8 75694 2100 75014 0.Dl5 1320000 530 1310000 2100 Footnotes For each contaminant the lower of the 15A NCAC 2L (2L) standard, interim standard, the USEPA non -zero MCLG, or the USEPA MCL was retained as the remediation goal. In cases where a 2L standard, interim standard, USEPA non-zero MCLG, or USEPA MCL were not available or sufficiently protective, the appropriate remediation goal was determined as per footnotes 5, 6, and 7. 2 All RG's Wlless otherwise specified by footnotes are the 15 NCAC 2L standard or interim standard. 3 USEPA MCL. 4 USEPAMCLG. 5 The RG is based on the carcinogenic endpoint for exposure through ingestion and inhalation (volatiles), and corresponds to an excess lifetime cancer risk of l .0E-06. 6 7 RG = 1.OE-06 x 25 550 days 350 days!year[(l .08 liters-yearlkg-day x slope factor oral kg-day/mg) +(1.08 liters-year/kg-day)(slope factor inhalation kg-day/mg)] For volatile carcinogens it is assumed that the amount of contaminant inhaled is equal to that of ingesting 2-liters of contaminated water a day (USEPA Region IV guidance). The RG is based on the carcinogenic endpoint for exposure through the ingestion route (non-volatile). RG obtained from USEPA Region Ill Risk-Based Concentration Table and corresponds to an excess lifetime cancer risk of l .0E-06. The RG is based on the non-carcinogenic endpoint for exposure through the ingestion route. RG = 0.2 X RID mg/kg/day x 70 kg body wt 2 liters water ingested/day (15 NCAC 2L equation for non-carcinogens) C -14 I I I I I I I] I I I I I I I I I I I I I I I I I .I I I I I I I I I I I I Attachment D: Sensitive Environment Contacts SENSITIVE ENVIRONMENT National Parks and Slate Parks Designated and Proposed Federal and State Wilderness and Natural Areas SOURCE OF INFORMATION NC Division of Parks and Recreation • Natural Heritage Program Sensitive Areas Identified Under the ~a_tional Estuary •. Program or the Near Coastal Waters Program Critical Areas Identified Under the Clean Lakes Program National and State Seashore, Lakeshore and River Recreational Areas Critical Habitats or Habitats Known to be Used by State or Federally Designated or Proposed Endangered or Threatened Species or Species Under Review as to Their Endangered or Threatened Status National and State Preserves and Forests National or State Wildlife Refuges Federal Land Designated for Protection of Natural Ecosystems Terrestrial Areas Utilized for Breeding by Large or Dense Aggregations of Animals Areas Important to Maintenance of Unique Biotic Communities State-Designated Areas for Protection or Maintenance of A uatic Life Marine Sanctuaries National Monuments National and State Historical Sites National and State Seashore, Lakeshore and River Recreational Areas State or Federal Designated Scenic or Wild Rivers NOAA US Park Service NC Department of Cultural Resources NC Division of Parks and Recreation -Planning and Development Section TELEPHONE# .. (919) 733-7)0 I . ' (202) 606-4126 (202) 343-7014 (919) 733-5722 (919) 846-9991 SENSITWE ENVIRONMENT SOURCE OF INFORMATION Areas Identified Under Coastal Protection Legislation NC Division of Coastal Management Coastal Barriers or Units of a Coastal Barrier Resow-ces System Spawning Areas Critical for the Maintenance of Fish/Shellfish Species within River, Lake or Coastal Tidal Waters Migratory Pathways and Feeding Areas Critical for Maintenance of Anadromous Fish Species within River Reaches or Areas in Lakes or Coastal Tidal Waters in which such Fish Spend Extended Periods of Time State Lands Designated for Wildlife or Game Management State-Designated Areas for Protection or Maintenance of A uatic Life Wetlands -(On site or adjacent to site) NC Wildlife Resow-ces Commission US Army Corps of Engineers D-2 TELEPHONE# (919) 733-2293 (919) 288-5738 (919) 847-1707 I I I I I I I 1-- 1 I I I I •• I I I I I l J I ~ J l r t ~ l t I I . Attachment E: Checklist for Independent Remedial Action Report The checklist below follows the organization of section 6.0. of the guidelines. Please indicate whether each item is included, and identify its location in the final report (section and page). Ttoni I ii\II Section 6.0 Item 1. · 1 2 3 4 5 6 7 8 9 10 11 12 13 Section 6.0 Item 2. 1 .. 2 3 4 5 6 7 \ .• ~ §1[,t,lritihilal'iio)<ii>"ciiiii' :• I± · ... 4:/ii:fifiiO.t:/sl<ifo',iI::['Pi~if' .. 1 lf---------+-"----------------t------------------l lf-----9-1-------'-----t--------1 10 ll---------ll-+----------------1--------------m 12 ,1--______ 1_3--1---------------+--------------D Section 6.0 Item 3. U----S_ec_t_io_n_6_.o_It_em_4_. +----------------1---------------' Section 6.0 Item 5. a. 11----------+------------------ll------------------; I 11------b·--------+-------I C. 11------d·-+--------+-------I e. lf------f-1---------t--------• (C:\WPWIN60\WPDOCS\GUIDEUNES\GUIOLNI0.96) g I * For any item marked "no," provide an explanation for why it is not submitted or is not applicable. I Signature of Responsible Party or Consultant Date I I I .- I E-2 I I P77?!"fmmfm:::e:rt::mzeswrr.,. 7:rtnrzt rs mus I I D I g I, I ( I 1• -1 REF. 40 FIT REPORT SITE INSPECTION PRIORITIZATION GEORGIA-PACIFIC CORPORATION HAROWOOO SAWMILL PLYMOUTH, WflSHIHGTOH CO. tlC NCO OOIO 813 592 I ' ' I. I I ' ., 'I 'Ii :I i ·I I I I I I I D u ID 11, I I I I •• 11 ~· ' □YNAMAC CORPORATION Environmental Services Peachtree Center Tower 230 Peachtree Slreet, N.W. Suite 500 Atlanta, GA 30303 Telephone: 404·681-0933 Fax: 404-681-0894 April 15, 1994 Mr. Narindar Kumar, Acting Chief Site Assessment Section U.S. EPA Region IV 345 Courtland Street, NE Atlanta, Georgia 30365 t,-'"''11. APR 181994 I REr;en,r:.o I fvlAY241994 l surERFUNr: ;:,1;:,i:.r1oN / Re: Work Assignment C04119 -Site Inspection Prioritization Report -Georgia-Pacific Corporation Hardwood Sawmill, Plymouth, Washington County, North Carolina Document Control No. C04119-SIP-LC-500 Dear Mr. Kumar: Enclosed please find the Site Inspection Prioritization Report for the Georgia-Pacific Corporation Hardwood Sawmill in Plymouth, Washington County, North Carolina. This report has been developed to partially fulfill the requirements for TES VIII Work Assignment No. C04119, Task 5. This submittal includes a site map, supporting reference materials and a CERCLA Eligibility Form. If you have any questions or comments, please contact either of us at (404) 681-0933. Sincerely, (j~-AM~~~ ~;1.RPO~N . ff1/' ) . q,'., /lf'11 (Jv:;!-;t./!'C v Y Critt nden , Site Manager Regional Manager Enclosures cc: Ken Meyer, EPA Region IV Project Manager (w/o enclosures) Jack Silvey, Dynamac TES Program Manager (w/o references) Earl Bozeman, EPA Region IV Acting Work Assignment Manager Katharine Siders Franklin, Dynamac Work Assignment Manager (w/o references) TES WA File Corporate Headquarters: The Dynamac Building, 2275 Research Bou1evard, Suite 500, Rockville, MO 20850-3268 I State of North Carolina · Department of Environment, 11 Health and Natural Resources II Division of Solid Waste Management James B. Hunt, Jr., Governor n Jonathan B. Howes, Secretary. William L. Meyer, Director I I D I 1, I I ' g D I I· I June 14, -~996 ___ . Ms. Cynthia Gurley NC CERCLA Project Officer US EPA Region IV Waste Division, 6th Floor 345 Coiirtland Street, NE · Atlanta, GA 30365 Subject: Site Inspection Prioritization -Revised Weyerhauser Co./Plymouth (NCD 991 278 540) Plymouth, Martin County, NC Dear Ms. Gurley: This revised report contains the findings of the Site Inspection Prioritization (SIP) of the Weyerhauser Co. /Plymouth site (NCD 991 278 540), located on State Road 1565, Plymouth, Martin County, North Carolina. Please refer to the original June 30, 1995 SIP report for all references, tables, and figures. The Weyerhauser Co. site is an active wood and paper products manufactui:ing facility .... ~-located on State Road 1565 in Plymouth, Martin County, NC. Weyerhauser has been in operation at this site since 1957 when the company merged .with the Kieckhefer-Eddy Co. who began operations at the site in 1937. The paper bleaching operation began at the site in the mid-1940's. The Wood Products Division of Weyerhauser produces finished lumber and plywood from raw pine and hardwoods. Since 1979, Weyerhauser has been treating lumber with a chromated copper arsenate process that produces approximately 1500 pounds of treatment sludge per quarter. --A collection system is used to capture excess treatment solution and sludge which is then shipped off-site to a RCRA disposal facility. A mercury cell chlorine plant was operational at the site from approximately 1952 to. 1965. Spent graphite electrodes and marble cells, having absorbed mercury during the chlorine production process, were disposed ofin an on-site landfill with other mill wastes. The exact quantity of mercury disposed of during this period is unknown. However, Weyerhauser Co. estimates range from 60 pounds to 11,000 pounds of mercury. A series ofU-drains in the floor of the building collected spilled process fluid and directed it toward a collection sump which in tum discharged to a drainage trench that emptied into the Roanoke River. The chlorine production building was demolished in 1987; approximately 1,300 tons of mercury contaminated soil and I P.O. Box 27687, . . Raleigh, North Carolina 27611-7687 Voice 919-733-4996 FAX 919-715-3605 An Equal Opportunity Affirmative Action Employer 50% recycled/10% post-consumer paper ~ I_~: 'I -~~ l,. I I I m ' D I 1, I I I •• D u D m I I Ms. Gurley June 14, 1996 Page2 debris was removed to the GSX hazardous waste landfill in Pinewood, South Carolina. The area of the former building was then backfilled with clean fill and capped with asphalt pavement. Mercury contaminated soils remain in place at a depth of approximately 4.5 feet below land surface due to a high water table. Three shallow (12 ft) monitoring wells were constructed in a triangular pattern around the area of the former chlorine building. Groundwater from the monitoring well between the former building and the river consistently reveals elevated levels-of-mercury. A ¥C ,,. background monitoring well is free of mercury contamination. ··--- From the time operations began at the facility, untreated process wastewater from the paper products division was originally discharged to the Roanoke River. _ During the period between the early l 960's and 1968, all untreated process wastewater was discharged to Welch Creek instead of the Roanoke River. Since 1968, all process wastewater except cooling water has been treated at an on-site secondary treatment facility prior to discharge. Wastewater is directed to two settling ponds where solids are allowed to settle out and removed for burning in the plants' steam boiler: Wastewater is then sent to an aeration basin and finally to a serpentine retention pond approximately 750 acres in size. During the period between 1968 to 1988, wastewater from the retention pond was discharged to Welch Creek. Since 1988, Weyerhauser has been discharging treated process wastewater to the Roanoke River at a point approximately 1/2-mile downstream of the facility . The Weyerhauser Paper Company currently holds an NPDES Permit (# 0000680) to discharge treated wastewater, non-contact cooling water, and storm water runoff to the Roanoke River. Under the permit, Weyerhauser has a discharge limit of 1.3 pg/I of dioxin and is required to sample its effluent quarterly. Weyerhauser's original NPDES Permit was issued in 1975. In 1985, a Site Inspection was conducted by the North Carolina Solid and Hazardous Waste Management Branch/CERCLA Unit. No sampling was conducted during the Site Inspection. A fish consumption advisory has been issued by the NC Division of Environmental Management for the Roanoke River and Welch Creek based on fish tissue samples collected in 1988 exhibiting high dioxin concentrations. Sampling for the Weyerhauser Co. SIP (June 19-20, 1995) focused on sediment and surface water samples collected from the Roanoke River which is a closed fishery and has significant wetland surface water pathway frontage. Sediment and surface water samples were also collected from Welch Creek. An off-site drinking water sample was collected from the nearest residential well located at the James Johnson residence; an on-site .drinking water sample was collected from Weyerhauser well #13. All samples were analyzed under the US. Environmental Protection Agency {EPA) Contract Laboratory Program {CLP). No further waste/source sampling was performed at the facility during the SIP. Prior sampling data indicates that the shallow groundwater aquifer and subsurface soils under the former chlorine production building have been impacted by a release of mercury. Elevated levels of dioxin/furan have also been found in fish tissue samples collected from the Roanoke River and Welch Creek below Weyerhauser discharge points. The laboratory analytical data for sediment samples collected from the surface water pathway during the SIP indicate that an observed release of mercury has occurred, as well as the same isomers of dioxin/furan detected in fish tissue. I I I I fi I Ms. Gurley June 14, 1996 Page3 The drinking water samples were found to be free of chemical contaminants. Based on the above factors, it is apparent that the site poses a threat to human health and the environment and is in need of additional action under CERCLNSARA. The Weyerhauser Co./Plymouth site is therefore recommended to receive a low priority status for an Expanded Site Inspection assignment. If you have any questions, please feel free to contact me at (919) 733-2801. Sincerely, G. Doug Rumford Hydrogeologist NC Superfund Section I I I I I I I I I I I I I I I I I MEMORANDUM TO: File FROM: G.Doug Rumford~ Hydrogeologist, NC Superfund DA TE: 1/3/97 REF. 42 SUBJECT: Georgia-Pacific Corp. Hardwood Sawmill Plymouth, Washington County, NC NCO 000 813 592 Telecon with Doward Jones Jr. On this day I spoke with Mr. Doward Jones Jr. (919-793-2312 w) to inquire about the property owned by the Boy Scouts of America located adjacent to the former hardwood sawmill and to Plymouth High School. Mr. Jones is the Assistant Scout Master for the Plymouth, NC Boy Scout Troop. According to Mr. Jones, this parcel property was donated by the Still family to the Boy Scouts of America some time around 1950. The Still family owned and operated the Atlas Plywood facility which was later sold to Georgia-Pacific Corporation. The property was wooded at the time the Boy Scouts to possession. A portion of the property was then cleared to allow the Boy Scout Troop to construct a building which they still use as a facility for weekly meetings. Mr. Jones also mentioned that approximately 4 acres of the Boy Scout Property were annexed . by the city to build Plymouth High School. ti'lfflRIT1iY¥¥' Ref. 4 3 Report No. 93-02 HEAVY METALS IN ORGANIC-RICH MUDS OF THE ALBEMARLE SOUND ESTUARINE SYSTEM January 1993 . I ; ALBEMARLE-PAMLICO ESTUARINE STUDY NC O,,partm0nt ot Environment, Health, end Natural Resources Envlronmentc/ Protection Agency Nallonal Estuary Program . PART E: RESULTS ·riJf:±': AREAS 01" CONCERN IN Xl!E ALBEMARLE SOUND ESTUARINE SYSTEM . -;·-···Figure El is an index map showing the location of all area maps used in the r.·.a-J-".' PART E: RESULTS section of this report. Table El is an outline of the specific ,regional areas and associated maps that will be the basis for presentation and ·~discussion of all analytical data through the remainder of this report. J';;;..:.o JJ~:}.-_:- 1 ':_. Lower Roanoke River Area one of the largest wood products facilities in the world is located on the 'banks of Welch Creek and the Lower. Roanoke River west of Plymouth. This ·industrial site has been operating since 1938 and today consists of 1200 acres, "·,.,.·;:,hich includes 750 acres of industrial waste water treatment ponds (Fig. E2). ' .,,.>-'originally, all industrial waste water from the facility was discharged directly ~1iito the Roanoke River. However, during the period between the early l960"s and c/1988, all industrial waste water was discharged directly into Welch Creek (near r ·•· ·_WEL-4 in Fig. E2). Beginning in 1968 all industrial waste water, except cooling ~water, was processed through a secondary treatment plant before being discharged ~•?into adjacent creek waters. Since 1988, the 55 million gallons per day of i•· · , , noncooling, industrial waste water has been discharged directly into the Roanoke ~7River through a diffuser pipe across the River bottom. Thie discharge pipe is g£1c:icated downstream of the plant site and slightly upstream of the mouth of Welch l1·creek. ~-:Jjt:i; In a site inspection report for North Carolina, Durway ( 1986) d·escribed ... , .. ~!h...t:1:tre~ ori-site areas where hazardous substances occur, or in the ·past have been · J\rgenerated or disposed of. There probably-· have been ·many different sources of ~M:"~.?umerou~ contaminants from this large and complex industrial facility over the "Jji:years. It is not known to what extent any or all of these historic sites could t;'_.Continue to be impacting the adjacent waterways. ·. These sites include the J.{.following: ;l_~:it~-.· "'}'!"• .,_l{;).· 1o, .... --~/ ~r- ~~: ~-:J;t .ri-f?·: ·c~;:. ~ '..,f · , .. 1. A wood treatment plant has been chromate copper arsenate sludge material is stored in drums and operating since 1979 and produces a as a by-product material. This waste removed from the site for disposal. 2. Considerable amounts of mercury were associated with various phases of the old chlorine plant that operated until 1968. Some waste mercury was volatilized, some was discharged directly into the River, and some was disposed of in the old on-site landfill. 3. An old landfill, situated on a 35 to 50 acre tract of low wetland, received much onsite chemical waste including mercury, until 1979 w_hen it was sealed. Welch Creek ./ The sediments within Welch Creek, a very small southern tributary to the • __ l\oanoke River (Fig. E2), are substantially or slightly enriched in all 15 trace ·;·;-_ elements ( Table E2). Thirteen of these trace elements are substantially enriched ~~ in multiple sample sites. Four elements have extremely high enrichments-with ~.maximum enrichment factors as follows: Cr= 156 X, Hg= 73 X, Ni= 20 X, and cu {;_ -9 -4 X the ATM, respectively). Seven of the ten samples analyzed in Welch Creek ,e ;. 97 I I sites with maximum enrichment factors as follows: Hg= 12.3 X, Cr= 4.0 X, As= 3.4 X, and Cu= 2.3 X the ATM. Mercury is substantially enriched (up to 12.3 X ATM) in two samples at one site (RKE-13) off the mouth of Canaby Creek, along ''I with arsenic, cobalt, chromium, copper, manganese, tin, titanium, and zinc. Since all other Roanoke River samples, except RKE-9 near the present industrial site, have Very low concentrations of mercury, it is assumed that there could be ,.1 a major source of metal contamination up canaby Creek. This Creek should be sampled and analyzed for heavy metals. Chromium and copper are slightly to substantially enriched (up to 4.0 X and ,· 2.3 X ATM, respectively} in eight and 14 Lower Roanoke River samples, ',ii respectively. All copper enrichment occurs downstream of the paper mill's new NPDES discharge site. Cobalt is substantially enriched in Welch Creek and is only slightly enriched in the Roanoke River in 21 of the 26 samples •. Arsenic is not enriched in Welch. Creek except for the surface sample at the mouth of the :I Creek; however, it is slightly to substantially enriched in 17 samples in the Roanoke River downstream of the paper mill discharge. I :I :I ' ii It appears that there are significant amounts of various trace elements within the sediments of the Lower Roanoke River system. However, the general concentrations are lower than in Welch Creek and the distribution patterns of these trace elements are somewhat irregular. ·The Roanoke River is dominated by rapidly fluctuating flow conditions and resulting processes of sedimentation that range from low energy during low flow conditions to high energy during high flow conditions. These environmental variations would cause major changes ·in processes of sediment deposition and erosion within the Roanoke River channel and could explain the erratic distribution patterns. Middle and Cashie Rivers Middle and Cashie Rivers are distributary channels of the Lower· Roanoke River that are situated north of the main channel (Fig. E2). The Cashie River has its own tributary drainage, however,-it is conne~ted to the Roanoke River by the Thoroughfare Channel. Chemical data for surface samples at three sites in the Middle River and two sites in the outermost Cashie River are summarized in Table E4. Manganese and titanium are enriched in all samples (up to 4.2 X and 1.9· X ATM, respectively), while arsenic and cobalt are enriched in eight and seven of the ten samples ( up to 2. 8 X and 2. 0 X ATM, respectively}. Chromium and vanadium are variably enriched at both sites in the Cashie River (up to l.7 X and 1.5 X ATM, respectively}. Inner Albemarle sound Area Inner Albemarle Sound extends from the mouth of the Lower Roanoke River with broad floodplain swampforests to the west to the embayed Chowan River estuary to the north, and eastward to the western sides of the Yeopim River on the north and Bull Bay on the south (Fig. ES}. Inner Albemarle Sound is relatively narrow, about 5 miles wide, compared to the middle and outer portions further to the east, which are between 10 to 15 miles wide. Both the Roanoke and Chowan River Drainage Basins (Fig. Bl} discharge directly into Inner Albemarle Sound, which is an irregularly flooded, fresh water, drowned-river estuarine system (Fig. Dl). Three water bodies are described within this area and include the Chowan River and Edenton Bay embayed estuaries, as well as Inner Albemarle 105 . I , ,. ': ~ ':.:1· ._? :·•~ .. - ·-·,.:·~· .. ,:;--.. :,,; ;;.:-~_ ~1• ··--· .;.-5 ). RECEIVED JAN 2 31996 I I I I UNITED STATES ENVIRONMENTAL PROTECTION AGENCY SUPERFUN0 SECTiOr: Region IV Environmental Services Division College Station Road, Athens, Ga. 30613 l****MEMORANDUM****** I DATE: 01/12/96 ,SUBJECT; Results 95-0294 I of Dioxin/Furan Analysis; GA PACIFIC CORP HDWD PLYMOUTH NC SAS NO: SPR I FROM: ~harles H. Hooper l::{)V\~ Chief, Laboratory Evlluation;Quality I TO: PAT DEROSA Assurance Section lttached are the results of analysis of samples collected as part of .the subject project. Is a result of the Quality Assurance Review, certain data qualifiers may have been placed on the data. Attached is a DATA QUALIFIER IEPORT which explains the reasons that these qualifiers were required. 'ff you have any questions please contact me. I ATTACHMENT I I I I I a I lo"~ ' 1010 I oo \ I I I I I I I I I I DATA QUALIFIER REPORT Project No.: 95-0294 Case No.: SPR No. : 44854 Site Name: GA PACIFIC HDWD Affected Samples Analyte All total congeners 95501 95502 95503 95504 95505 95507 95508 95509 2378 TCDD 2378 TCDF 2378 TCDD 2378 TCDD 2378 TCDD OCDD 2378 TCDD OCDD 2378 TCDD 123678 HxCDD 1234678 HpCDD OCDD 2378 TCDF OCDF 2378 TCDD 123678 HxCDD 1234678 HpCDD OCDD OCDF I 2378 TCDD i 123678 HxCDD 1234678 HpCDD OCDD 2378 TCDF OCDF Flag Used J J J J J J J J J J J J J J J J J J J J J J J J J J Reason Assumed Resp. Factors/ Cal. Stds not available for all congeners high spike recovery low IS recovery high spike recovery high spike recovery high spike recovery 2 high spike recovery 2 high spike recovery 2 2 2 2 2 high spike recovery 2 2 2 2 high spike recovery 2 2 2 2 2 I I I I I I I I I I I I I I I I I I 95510 2378 TCDD J high spike recovery 1234678 HpCDD ·J 2 OCDD J 2 2378 TCDF J 2 OCDF J 2 95511 2378 TCDD J high spike recovery 95512 2378 TCDD J high spike recovery 123678 HxCDD J 2 1234678 HpCDD J 2 OCDD J 2 2378 TCDF J 2 OCDF J 2 TEQ's : The Toxic Equivalent (TEQ} represents a surrnnation of values from the individual equivalents that are calculated for each of the 2, 3, 7, 8 contain.ing isomers·. If 10% or greater of the total value was from data considered to be estimated, then the TEQ is reported as estimated {J flag}. Abbreviation Key: TCDD = Tetrachlorodi~nzodioxin PeCDD = Penta 11 11 11 TCDF = Tetrachlorodibenzofuran PeCDF = Penta 11 11 11 11 HxCDD = Hexa 11 11 11 HxCDF = Hexa 11 11 n 11 HpCDD = Hepta II i ;, 11 HpCDF = Hepta 11 11 11 11 OCDD Octa 11 11 11 OCDF = Octa 11 11 11 11 Reason Codes l. Results lower than the minimum quantitation limit 2. Results higher than the maximum calibration limit 3. Poor precision on the 2,3,7,8-TCDF confirmation column ---- ---liiiiia &iiiil· 01/11/96 - -l!!!l!l!!!I I!!!!!! 1!!11!1 SAMPLE AND"""'im"ALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. DIOXIN/FURAN DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0294 SAMPLE NO. 95501 SAMPLE TYPE, SOIL SOURCE, GA PACIFIC CORP HDWD STATION ID, 009-SD CASE NUMBER, 0 SAS NUMBER, SPR PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 D NUMBER, 009SD - BY, D RUMFORD ST, NC 1425 STOP, 00/00/00 ** ** ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** NG/KG 23J 30U 3.0 20UJ 10U 20U 10U 110UJ 310U 950UJ 4000U 190J 300J 2.5U ANALYTICAL RESULTS 2,3,7,8 TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN(TOTAL) OCTACHLORODIBENZODIOXIN(TOTAL) 2,3,7,8 TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZOFURAN ***FOOTNOTES*** NG/KG lOU 50UJ 2.5U 10U 2.5U 10U 90UJ 60U 2.5U 150UJ 90U 44 59 ANALYTICAL RESULTS 2,3,4,7,8 PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZOFURAN 1,2,3,6,7,8 HEXACHLORODIBENZOFURAN 1,2,3,7,8,9 HEXACHLORODIBENZOFURAN 2,3,4,6,7,8 HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN 1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN(TOTAL) OCTACHLORODIBENZOFURAN(TOTAL) TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89) % MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -- --DIOXIN/FURAN DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * •• ** ** ** ** PROJECT NO. 95-0294 SAMPLE NO. 95502 SAMPLE TYPE, SOIL SOURCE, GA PACIFIC CORP HDWD STATION ID, 010-SD CASE NUMBER, 0 SAS NUMBER, SPR PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 D NUMBER, OlOSD BY, D RUMFORD ST, NC 1620 STOP, 00/00/00 ==-= 01/11/96 * * * * *** ** •• •• ** •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** NG/KG 5.8J lOUJ 2.5U lOUJ 2.5U 20U lOU 70UJ 480U 980UJ 4100U 53 lOOUJ 2.SU ANALYTICAL RESULTS 2,3,7,8 TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN(TOTAL) OCTACHLORODIBENZODIOXIN(TOTAL) 2,3,7,8 TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZOFURAN ***FOOTNOTES*** NG/KG 2.5U 20UJ 2.5U 2.5U 2.5U 2.5U 40UJ 40U 2.5U llOUJ llOU 11 48 ANALYTICAL RESULTS 2,3,4,7,8 PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZOFURAN 1,2,3,6,7,8 HEXACHLORODIBENZOFURAN 1,2,3,7,8,9 HEXACHLORODIBENZOFURAN 2,3,4,6,7,8 HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN 1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN(TOTAL) OCTACHLORODIBENZOFURAN(TOTAL) TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89) % MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. --·--· -----· -EPA-REGION IV ESD, ATHENS, GA. 01/11/96 DIOXIN/FURAN DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0294 SAMPLE NO. 95503 SAMPLE TYPE, SOIL SOURCE, GA PACIFIC CORP HDWD STATION ID, 109-SD CASE NUMBER, 0 SAS NUMBER, SPR PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 D NUMBER, 109SD / BY, D RUMFORD ST, NC 1425 STOP, 00/00/00 ** ** ** ** •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * **• NG/KG 24J 40UJ 5.0J 30UJ 25U 120U 30U 490UJ 2100U 3900UJ 18000 200 380J 25U ANALYTICAL RESULTS 2,3,7,8 TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN(TOTAL) OCTACHLORODIBENZODIOXIN(TOTAL) 2,3,7,8 TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZOFURAN ***FOOTNOTES*** NG/KG 25U 250UJ 25U 25U 25U 25U 410UJ 260U 25U 780UJ 470U 64 58 ANALYTICAL RESULTS 2,3,4,7,8 PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZOFURAN 1,2,3,6,7,8 HEXACHLORODIBENZOFURAN 1,2,3,7,8,9 HEXACHLORODIBENZOFURAN 2,3,4,6,7,8 HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN 1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN(TOTAL) OCTACHLORODIBENZOFURAN(TOTAL) TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89) % MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. ----.. -sil'1! AN~LY~ .. MANA-NT -EM -11!!1!!!1 DIOXIN/FORAN DATA REPORT EPA-REGION IV ESD, ATHENS, GA. *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ** ** ** ** ** PROJECT NO. 95-0294 SAMPLE NO. 95504 SAMPLE TYPE, SOIL SOURCE, GA PACIFIC CORP HDWD STATION ID, 001-SD CASE NUMBER, 0 SAS NUMBER, SPR PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D NUMBER: 00lSD,, BY, D RUMFORD ST, NC 1020 STOP, 00/00/00 ... -01/11/96 * * * * *** ** ** ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** NG/KG 23J 30UJ 3.5 30UJ lOU 60U 20U 250UJ 990U 2300U 5600J 200 370J lOU ANALYTICAL RESULTS 2,3,7,8 TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN .1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN(TOTAL) OCTACHLORODIBENZODIOXIN(TOTAL) 2,3,7,8 TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZOFURAN ***FOOTNOTES*** NG/KG 20U SOUJ lOU 6.0U 2.5U lOU 240UJ 110U lOU 340UJ 150U 45 56 ANALYTICAL RESULTS 2,3,4,7,8 PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZOFURAN 1,2,3,6,7,8 HEXACHLORODIBENZOFURAN 1,2,3,7,8,9 HEXACHLORODIBENZOFURAN 2,3,4,6,7,8 HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN 1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN(TOTAL) OCTACHLORODIBENZOFURAN(TOTAL) TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89) % MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -- - -DIOXIN/FURAN DATA REPORT *** * * * * * * * * * * * * * * * ** •• ** ** ** PROJECT NO. 95-0294 SAMPLE SOURCE, GA PACIFIC CORP HDWD STATION ID, 002-SL CASE NUMBER, 0 ---11!!!!1 -I!!!!!!!!!! SAMPLE AND ANALYSIS MANAGEMENT EPA-REGION IV ESD, ATHENS, * * * * * * * * * * * * * * * * * * * * * * * l!!l!l!!I SYSTEM GA. * * * 1!!!!111 * * * * * NO. 95505 SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 SAS NUMBER, SPR D NUMBER, 002SL.,... * * * * • • • BY, D RUMFORD ST, NC 1155 STOP, • • • • • 00/00/00 • • == 01/11/96. • • • •• •• •• •• •• •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** NG/KG 19J 50UJ 170 650J 220 830 500 4600J 16000 32000J 92000J 30U BOUJ 30U ANALYTICAL RESULTS 2, 3; 7, 8 TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN(TOTAL) OCTACHLORODIBENZODIOXIN(TOTAL) 2,3,7,8 TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZOFURAN ***FOOTNOTES*** NG/KG BOU 500UJ 59 90U 36 120 2100J 1400 81 4000J 1500 550J 50 ANALYTICAL RESULTS 2,3,4,7,8 PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZOFURAN 1,2,3,6,7,8 HEXACHLORODIBENZOFURAN 1,2,3,7,8,9 HEXACHLORODIBENZOFURAN 2,3,4,6,7,8 HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN 1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN(TOTAL) OCTACHLORODIBENZOFURAN(TOTAL) TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89) % MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. ,' - ---- -DIOXIN/FORAN DATA REPORT I -iiil iiiiiil iiil SAMPLE AND ANALYSIS MANAGEMENT EPA-REGION IV ESD, ATHENS, iiiiii SYSTEM GA, lliiii liiiiiii1 == l!!l!I 01/11/96 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO, 95-0294 SAMPLE NO, 95506 SAMPLE TYPE, SOIL SOURCE, GA PACIFIC CORP HDWD STATION ID, 003-SL CASE NUMBER, 0 SAS NUMBER, SPR PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D NUMBER, 003SL, BY, D RUMFORD ST, NC 0950 STOP, 00/00/00 ** ** ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** NG/KG 2,5U 2,5UJ 2,5U 10UJ 2,5U 10U 10U 50UJ 220U 540UJ 4900U 2,5U 3,0UJ 2,5U ANALYTICAL RESULTS 2,3,7,8 TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN(TOTAL) OCTACHLORODIBENZODIOXIN(TOTAL) 2,3,7,8 TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZOFURAN ***FOOTNOTES*** NG/KG 2,SU 10UJ 2,5U 2,5U 2,5U 2,5U 30UJ 20U 2,5U 50UJ 30U 0 22 ANALYTICAL RESULTS 2,3,4,7,8 PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZOFURAN 1,2,3,6,7,8 HEXACHLORODIBENZOFURAN 1,2,3,7,8,9 HEXACHLORODIBENZOFURAN 2,3,4,6,7,8 HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN 1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN(TOTAL) OCTACHLORODIBENZOFURAN(TOTAL) TEQ(TOXIC, EQUIV, VALUE, FROM I-TEF/89) % MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED, THE NUMBER IS THE MINIMUM QUANTITATION LIMIT, *R-QC INDICATES THAT DATA UNUSABLE, COMPOUND MAY OR MAY NOT BE PRESENT, RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION, -- - - ------SAMPLE AND ANALYSIS MANAGEMENT -SYSTEM -- -- --EPA-REGION IV ESD, ATHENS, GA. 01/11/96 DIOXIN/FURAN DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0294 SAMPLE NO. 95507 SAMPLE TYPE, SOIL SOURCE, GA PACIFIC CORP HDWD STATION ID, 004-SL CASE NUMBER, 0 SAS NUMBER, SPR PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D NUMBER: 004SL ,,, BY, D RUMFORD ST, NC 1125 STOP, 00/00/00 ** ** ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** NG/KG 82J 260J 1500 22000J 5000 43000J 7400 160000J 320000J 620000J 370000J 300 2600J 480 ANALYTICAL RESULTS 2,3,7,8 TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN(TOTAL) OCTACHLORODIBENZODIOXIN(TOTAL) 2,3,7,8 TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZOFURAN ***FOOTNOTES*** NG/KG 86 33000J 3600 1700U 1400 3700 140000J 81000U 10000 9800J 90000J llOOOJ 18 ANALYTICAL RESULTS 2,3,4,7,8 PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZOFURAN 1,2,3,6,7,8 HEXACHLORODIBENZOFURAN 1,2,3,7,8,9 HEXACHLORODIBENZOFURAN 2,3,4,6,7,8 HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN 1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN(TOTAL) OCTACHLORODIBENZOFURAN(TOTAL) TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89) % MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. . !!!!!. == liiiiil liiii -----EPA-REGION IV ESD, ATHENS, GA. 01/11/96 DIOXIN/FURAN DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0294 SAMPLE NO. 95508 SAMPLE TYPE, SOIL SOURCE, GA PACIFIC CORP HDWD STATION ID, 005-SL CASE NUMBER, 0 SAS NUMBER, SPR PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D NUMBER, OOSSL - BY, D RUMFORD ST, NC 1020 STOP, 00/00/00 ** ** ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** NG/KG 180J 420J 2900 22000J 4100 4SOOOJ 11000 180000J 120000J 230000J 360000J 660 6500J 910 ANALYTICAL RESULTS 2,3,7,8 TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN(TOTAL) OCTACHLORODIBENZODIOXIN(TOTAL) 2,3,7,8 TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZOFURAN ***FOOTNOTES*** NG/KG 4100 80000J 2900 4100U 1900 6100 140000J 46000U 4000 3800J 120000J 13000J 41 ANALYTICAL RESULTS 2,3,4,7,8 PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZOFURAN 1,2,3,6,7,8 HEXACHLORODIBENZOFURAN 1,2,3,7,8,9 HEXACHLORODIBENZOFURAN 2,3,4,6,7,8 HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN 1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN(TOTAL) OCTACHLORODIBENZOFURAN(TOTAL) TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89) % MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFic;ATION. !!!!I i:;;;a liiii DIOXIN/FURAN DATA REPORT -iiiii - - SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. -- -- --01/11/96 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * *· * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *· * * * *** ** ** ** ** ** PROJECT NO. 95-0294 SAMPLE NO. 95509 SAMPLE TYPE, SOIL SOURCE, GA PACIFIC CORP HDWD STATION ID, 006-SL CASE NUMBER, 0 SAS NUMBER, SPR PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D NUMBER, 006SL / BY, D RUMFORD ST, NC 1040 STOP, 00/00/00 ** ** •• •• ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** NG/KG 1100J 4200J 18000 200000J 50000 1100000J · 99000 3000000J 8300000J 1.4E7 2.6E7 8000J 32000J 18000 ANALYTICAL RESULTS 2,3,7,8 TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN(TOTAL) OCTACHLORODIBENZODIOXIN(TOTAL) 2,3,7,8 TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZOFURAN ***FOOTNOTES*** NG/KG 37000 460000J 100000 42000U 55000 86000 3700000J 2200000U 230000 220000J 1. 3E7 300000J 56 ANALYTICAL RESULTS 2,3,4,7,8 PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZOFURAN 1,2,3,6,7,8 HEXACHLORODIBENZOFURAN 1,2,3,7,8,9 HEXACHLORODIBENZOFURAN 2,3,4,6,7,8 HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN 1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN(TOTAL) OCTACHLORODIBENZOFURAN(TOTAL) TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89) % MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. ;;;;;a liiiiiil liiii -· ---- - - - SAMPLE AND ANALYSIS MANAGEMENT SYSTEM ----DIOXIN/FURAN DATA REPORT EPA-REGION IV ESD, ATHENS, GA. 01/11/96 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *· * * * *** •• •• •• •• •• PROJECT NO. 95-0294 SAMPLE NO. 95510 SAMPLE TYPE, SOIL SOURCE, GA PACIFIC CORP HDWD STATION ID, 007-SL CASE NUMBER, 0 SAS NUMBER, SPR PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D NUMBER, 007SL' BY, D RUMFORD ST, NC 0900 STOP, 00/00/00 •• •• •• •• • • *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** NG/KG 2200J 4300J 28000 140000J 67000 990000 140000 2900000J 8400000J 1. SE? 2.9E7 13000J 62000J 20000 ANALYTICAL RESULTS 2,3,7,8 TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN(TOTAL) OCTACHLORODIBENZODIOXIN(TOTAL) 2,3,7,8 TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZOFURAN ***FOOTNOTES*** NG/KG 40000 SOOOOOJ 94000 47000 56000 79000 3200000J 1800000U 200000 6000000J 1. 3E7 310000J 57 ANALYTICAL RESULTS 2,3,4,7,8 PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZOFURAN 1,2,3,6,7,8 HEXACHLORODIBENZOFURAN 1,2,3,7,8,9 HEXACHLORODIBENZOFURAN 2,3,4,6,7,8 HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN 1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN(TOTAL) .OCTACHLORODIBENZOFURAN(TOTAL) TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89) % MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. --I!!!!! 9= sffl mffiALYS.MANA-~ ~EM -. -. ---.. EPA-REGION IV ESD, ATHENS, GA. 01/11/96 DIOXIN/FURAN DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0294 SAMPLE NO. 95511 SAMPLE TYPE, SOIL SOURCE, GA PACIFIC CORP HDWD STATION ID, 101-SD CASE NUMBER, 0 SAS NUMBER, SPR PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D NUMBER, 101SD- BY, D RUMFORD ST, NC 1020 STOP, 00/00/00 ** ** ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** NG/KG 13J 20UJ 3.4 30UJ 5.3 70U 20U 240UJ 1400U 2600UJ 5100U 120 230J 10U ANALYTICAL RESULTS 2,3,7,8 TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN(TOTAL) OCTACHLORODIBENZODIOXIN(TOTAL) 2,3,7,8 TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZOFURAN ***FOOTNOTES*** NG/KG 10U 40UJ 2.5U 2.5U 10U 10U 250UJ 180U 10U 600UJ 280U 27 56 ANALYTICAL RESULTS 2,3,4,7,8 PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZOFURAN 1,2,3,6,7,8 HEXACHLORODIBENZOFURAN 1,2,3,7,8,9 HEXACHLORODIBENZOFURAN 2,3,4,6,7,8 HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN 1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN(TOTAL) OCTACHLORODIBENZOFURAN(TOTAL) TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89) % MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -I!!!!!! !II!! -. == Iii.a iiiii -liiiil. -SAMPLE AND ANALYSIS MANAGEMENT SYSTEM - --·-- -DIOXIN/FURAN DATA REPORT EPA-REGION IV ESD, ATHENS, GA. 01/11/96 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *-* * * *** •• •• •• •• •• PROJECT NO. 95-0294 SAMPLE NO. 95512 SAMPLE TYPE, SOIL SOURCE, GA PACIFIC CORP HDWD STATION ID, 107-SL CASE NUMBER, 0 SAS NUMBER, SPR PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D NUMBER, 107SL - BY, D RUMFORD ST, NC 0900 STOP, 00/00/00 •• •• •• •• • • *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** NG/KG 1400J 8100J 20000 120000J 52000 1200000J 110000 3200000J l.OE7 1. 6E7 3. 9E7 16000J 95000J 23000 ANALYTICAL RESULTS 2,3,7,8 TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,7;8 HEXACHLORODIBENZODIOXIN 1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN(TOTAL) OCTACHLORODIBENZODIOXIN(TOTAL) 2,3,7,8 TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN(TOTAL) 1,2,3,7,8 PENTACHLORODIBENZOFURAN ***FOOTNOTES*** NG/KG 70000 750000J 95000 40000U 60000 79000 3600000J 2000000U ·200000 7800000J l.7E7 370000J 58 ANALYTICAL RESULTS 2,3,4,7,8 PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,7,8 HEXACHLORODIBENZOFURAN 1,2,3,6,7,8 HEXACHLORODIBENZOFURAN 1,2,3,7,8,9 HEXACHLORODIBENZOFURAN 2,3,4,6,7,8 HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN 1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN(TOTAL) OCTACHLORODIBENZOFURAN(TOTAL) TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89) % MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. I I I I UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region IV Environmental Services Division College Station Road, Athens, Ga. 30613 l***MEMORANDUM****** I DATE: 08/16/95 SUBJECT: I D FROM: Results 95-0293 of Extractable Organic Analysis; GA PACIFIC CORP HDWD PLYMOUTH NC ~SE NO: 23679 ar es·H~~'jv hief, Laboratory Evaluation/Quality Assurance Section u u TO: PAT DEROSA Attached are the results of analysis of samples collected as part of jfe subject project. It a result of the Quality Assurance Review, certain data qualifiers may have been placed on the data. Attached is a DATA QUALIFIER 'PORT which explains the reasons that these qualifiers were required. If you have any questions please contact me. I I I I I ATTACHMENT I I I I I I I I I I g D D I ORGANIC DATA QUALIFIER REPORT Case Number 23679 Project Number 95-0293 SAS Number Site ID. Georgia Pacific Corp HDWD, Plymouth, NC Affected Samples Volatiles all samples 95446 95447,95453, 95455 Extractables 95445,95446 95447,95450, 95452,95454, 95456, 95458, I 95460,95462 95448 95451 oo-Z 95453,95455, 95459 95455 95457 95461 Compound or Fraction chloromethane benzene toluene chlorobenzene 2-butanone all compounds pyrene benzo(g,h,i)perylene pyrene di-n-octylphthalate benzo(b/k)fluoranthene benzo(a)pyrene indeno(l,2,3-cd)pyrene dibenz(a,h)anthracene benzo(g,h,t)perylene pyrene benzo(b/k)fluoranthene benzo(g,h,i)perylene fluoranthene pyrene benzo(b/k)fluoranthene benzo(g,h,i)perylene benzo(a)pyrene chrysene phenanthrene fluoranthene pyrene chrysene benzo(a)pyrene indeno(l,2,3-cd)pyrene benzo(g,h,i)perylene fluoranthene pyrene chrysene benzo(b/k)fluoranthene benzo(a)pyrene benzo(g,h,i)perylene R J J J J J J J J J Flag Used J J J J J J J J J J J J J J J J J J J J J J J J J J J Reason unacceptable PE sample recovery < quantitation limit < quantitation limit < quantitation limit < quantitation limit exceeded extraction holding time low PE sample recovery low PE sample recovery low PE sample recovery low internal standard recovery low internal standard recovery low internal standard recovery low internal standard recovery low internal standard recovery low internal .standard recovery < quantitation limit < quantitation limit low PE sample recovery < quantitation limit < quantitation limit < quantitation limit low PE sample recovery < quantitation limit < quantitation limit < quantitation limit < qunatitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit low PE sample recovery I I I I I I I I I D D I I ORGANIC DATA QUALIFIER REPORT Case Number 23679 Affected Samples Compound or Fraction Pesticides all samples ' 95445,95446 95447 95454 95455 95457 95459 aroclor-1016 alpha-bhc delta-bhc gamma-bhc 4,4'-DDE 4,4' -DDT beta-bhc 4,4'-DDE delta-bhc gamma-bhc endrin aldehyde 4,4':DDE Project Number 95-0293 Flag Used R C C C J J J J J N J J J N Reason unacceptable PE sample recovery GC/MS confirmed GC/MS confirmed GC/MS confirmed < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit difference in column quantitations < quantitation limit < quantitation limit < quantitation limit difference in column quantitations EXTRACTABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM · EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** *. * * * * * * *. * * * * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * *** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95445 SOURCE, GA PACIFIC CORP HDWD STATION ID, 007-SL / ** CASE NO.: 23679 SAMPLE TYPE, SOIL SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NO., KA86 BY, D RUMFORD ST, NC 0900 STOP, 00/00/00 ** ** ** ** ** *** * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 4800J 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 2800J 6800J 24000UJ 61000UJ 24000UJ 24000UJ 24000UJ ANALYTICAL RESULTS PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL 2,2'-CHLOROISOPROPYLETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISO PHO RONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY) METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE ***REMARKS*** EXCESSIVE HOLDING TIME ***FOOTNOTES*** UG/KG 61000UJ 24000UJ 61000UJ 61000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 61000UJ 61000UJ 24000UJ 24000UJ 24000UJ 2l+E06J 24000UJ 24000UJ 24000UJ 24000UJ 9400J 97000J 24000UJ 24000UJ 24000UJ 16000J 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 59 ANALYTICAL RESULTS 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHI)PERYLENE PERCENT MOISTURE ***REMARKS*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-M!>.TERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R0 QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. --l!!!!!!!I l!!!l!I 1!!!!!111 liiliil ----- -- --- EXTRACTABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95446 SOURCE, GA PACIFIC CORP HDWD STATION ID, 107-SL ** CASE NO.: 23679 SAMPLE TYPE, SOIL SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NO., KA87 BY, D RUMFORD ST, NC 0900 STOP, 00/00/00 ** ** ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ ·24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 61000UJ 24000UJ 61000UJ 24000UJ 24000UJ 24000UJ ANALYTICAL RESULTS PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL 2,2'-CHLOROISOPROPYLETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY) METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE ***REMARKS*** EXCESSIVE HOLDING TIME ***FOOTNOTES*** UG/KG 61000UJ 24000UJ 61000UJ 61000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 61000UJ 61000UJ. 24000UJ 24000UJ 24000UJ 24+E06J 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 6800J 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 24000UJ 63 ANALYTICAL RESULTS 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE . CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHI)PERYLENE PERCENT MOISTURE ***REMARKS*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -I!!!!!!! l!!!!!!!I - - ------ EXTRACTABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * •• * * * * * *. * * * * * * * * * * *. * * * * * * * * * * * *** •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95447 SOURCE, GA PACIFIC CORP HDWD STATION ID, 003-SL ~ ** CASE NO.: 23679 SAMPLE TYPE, SOIL SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NO., KA88 BY, D RUMFORD ST, NC 0950 STOP, 00/00/00 •• ** • • ** •• *** * * * * * * ••• * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * *. *** UG/KG 410U 410U 410U 410U 410U 410U 410U 410U 410U 410U 410U 410U 410U 410U 410U 410U 410U 410U 410U 410U 410U 410U 410U 410U 410U 1000U 410U 1000U 410U 410U 410U ANALYTICAL RESULTS PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,.4 -DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL 2,2'-CHLOROISOPROPYLETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISO PHO RONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY) METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE ***FOOTNOTES*** UG/KG 1000U 4100 10000 10000 4100 4100 4100 4100 4100 10000 10000 4100 4100 4100 24000 4100 4100 4100 4100 4100 410UJ 4100 410U 4100 4100 4100 4100 4100 4100 410U 4100 410UJ 21 ANALYTICAL RESULTS 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4 -NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHI)PERYLENE PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -l!!!!!!!I l!!!!!!l!I 111!!!!!!1 l!!!l!!I == . ==. ;;;a liiiil llii EXTRACTABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * •• * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95448 SOURCE, GA PACIFIC CORP HDWD STATION ID, 005-SL, ** CASE NO.: 23679 SAMPLE TYPE, SOIL SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NO., KA89 BY, D RUMFORD ST, NC 1020 STOP, 00/00/00 •• •• • • •• •• *** * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG 550U 550U 550U 550U 550U 550U 550U 550U 550U 550U 550U 550U 550U 550U 550U 550U 550U 550U 550U 550U 550U 550U 550U 550U 550U 1400U 550U 1400U 550U 550U. 550U ANALYTICAL RESULTS PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1, 3-DICHLOROBENZENE. 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL 2,2'-CHLOROISOPROPYLETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY) METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE ***FOOTNOTES*** UG/KG 1400U 550U 1400U 1400U 550U 550U 550U 550U 550U 1400U 1400U 550U 550U 550U 1400U 550U 550U 550U 550U 550U 550UJ 550U 550U 550U 550U 550U -550UJ 550UJ 550UJ 550UJ 550UJ 550UJ 40 ANALYTICAL RESULTS 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHI)PERYLENE PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-M.;TERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. l!!!!!I 1!!11111 == iilii iiiiil ----- --- --- EXTRACTABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * *. * * * * * * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * *** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95449 SOURCE, GA PACIFIC CORP HDWD STATION ID, 006-SL • ** CASE NO.: 23679 SAMPLE TYPE, SOIL SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NO., KA90 BY, D RUMFORD ST, NC 1040 STOP, 00/00/00 ** ** ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG ANALYTICAL RESULTS NA PHENOL NA BIS(2-CHLOROETHYL) ETHER NA 2-CHLOROPHENOL NA 1,3-DICHLOROBENZENE NA 1,4-DICHLOROBENZENE NA 1,2-DICHLOROBENZENE NA. 2-METHYLPHENOL NA 2,2'-CHLOROISOPROPYLETHER NA (3-AND/OR 4-)METHYLPHENOL NA N-NITROSODI-N-PROPYLAMINE NA HEXACHLOROETHANE NA NITROBENZENE NA ISOPHORONE NA 2-NITROPHENOL NA 2,4-DIMETHYLPHENOL NA BIS(2-CHLOROETHOXY) METHANE NA 2,4-DICHLOROPHENOL NA 1,2,4-TRICHLOROBENZENE NA NAPHTHALENE NA 4-CHLOROANILINE NA HEXACHLOROBUTADIENE NA 4-CHLOR0-3-METHYLPHENOL NA 2-METHYLNAPHTHALENE NA HEXACHLOROCYCLOPENTADIENE (HCCP) NA 2,4,6-TRICHLOROPHENOL NA 2,4,5-TRICHLOROPHENOL NA 2-CHLORONAPHTHALENE NA 2-NITROANILINE NA DIMETHYL PHTHALATE NA ACENAPHTHYLENE NA 2,6-DINITROTOLUENE ***REMARKS*** NO SAMPLE CONTAINER RECEIVED ***FOOTNOTES*** UG/KG ANALYTICAL RESULTS NA 3-NITROANILINE NA ACENAPHTHENE NA 2,4-DINITROPHENOL NA 4-NITROPHENOL NA DIBENZOFURAN NA 2,4-DINITROTOLUENE NA DIETHYL PHTHALATE NA 4-CHLOROPHENYL PHENYL ETHER NA FLUORENE NA 4-NITROANILINE NA 2-METHYL-4,6-DINITROPHENOL NA N-NITROSODIPHENYLAMINE/DIPHENYLAMINE NA 4-BROMOPHENYL PHENYL ETHER NA HEXACHLOROBENZENE (HCB) NA PENTACHLOROPHENOL NA PHENANTHRENE NA ANTHRACENE NA CARBAZOLE NA DI-N-BUTYLPHTHALATE NA FLUORANTHENE NA PYRENE NA BENZYL BUTYL PHTHALATE NA 3,3'-DICHLOROBENZIDINE NA BENZO(A)ANTHRACENE NA CHRYSENE NA BIS(2-ETHYLHEXYL) PHTHALATE NA DI-N-OCTYLPHTHALATE NA BENZO(B AND/OR K)FLUORANTHENE NA BENZO-A-PYRENE NA INDENO (1,2,3-CD) PYRENE NA DIBENZO(A,H)ANTHRACENE NA BENZO(GHI)PERYLENE PERCENT MOISTURE ***REMARKS*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MJ\.TERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. iilllii ------- ---- ----• I EXTRACTABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ·ATHENS, GA. . 08/15/95 *** * * *. * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * * * *** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 954.50 SOURCE, GA PACIFIC CORP HDWD STATION ID, 001-SW, ** CASE NO.: 23679 SAMPLE TYPE, SURFACEWA SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NO., KA91 BY, D RUMFORD ST, NC 1015 STOP, 00/00/00 ** ** ** ** ** *** * * * *. * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * *** UG/L lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU 25U lOU 25U lOU lOU lOU ANALYTICAL RESULTS PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL 2,2'-CHLOROISOPROPYLETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY) METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE ***FOOTNOTES*** UG/L 25U lOU 25U 25U lOU lOU lOU lOU lOU 25U 25U lOU lOU lOU 25U lOU lOU lOU lOU lOU lOUJ lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOUJ ANALYTICAL RESULTS 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHI)PERYLENE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-M.b.TERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. ------1!!11!!1 !!Ill == liiilil iiii - EXTRACTABLE ORGANICS DATA REPORT BAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95451 SOURCE: GA PACIFIC CORP HDWD STATION ID: 001-SD, ** CASE NO.: 23679 SAMPLE TYPE: SOIL SAS NO.: PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/20/95 D. NO.: KA92 BY:· D RUMFORD ST: NC 1020 STOP: 00/00/00 •• •• • • •• •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG B20U 820U 820U B20U 820U 820U 820U 820U 820U 820U 820U 820U 820U 820U 820U 820U 820U 820U 820U 820U 820U 820U 820U 820U 820U 2100U 820U 2100U 820U 820U 820U ANALYTICAL RESULTS PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL 2,2'-CHLOROISOPROPYLETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY) METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE ***FOOTNOTES*** UG/KG 2100U 820U 2100U 21000 820U 820U 820U 820U 820U 21000 21000 820U 820U 820U 19000 820U 820U 820U 820U 820U lBOJ 820U 820U 820U 820U 820U 820U 120J 820U 820U 820U 820UJ 60 ANALYTICAL RESULTS 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHI)PERYLENE PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -- - l!!!!I == ;;;a . liiiil ---- - - . ' EXTRACTABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * *. * * * * •. * * * * * * * * *** •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95452 SOURCE, GA PACIFIC CORP HDWD STATION ID, 101-SW ** CASE NO.: 23679 SAMPLE TYPE, SURFACEWA SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NO., KA93 BY, D RUMFORD ST, NC 1015 STOP, 00/00/00 •• •• • • •• •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU 25U lOU 25U lOU lOU lOU ANALYTICAL RESULTS PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL 2,2'-CHLOROISOPROPYLETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISO PHO RONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY) METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2, 4, 5-.TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE ***FOOTNOTES*** UG/L 25U lOU 25U 25U lOU lOU lOU lOU lOU 25U 25U lOU lOU lOU 25U lOU lOU lOU lOU lOU lOUJ lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOUJ ANALYTICAL RESULTS 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER ·FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHI)PERYLENE *A-AVERAGE VALUE *NA-NOT ANALYZED . *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS rs NECESSARY FOR VERIFICATION. ti!!!!! ----a;; "liiiil ----- ---- - -- EXTRACTABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * •• * •••• * •• *. * * *. * *. *. * *. * •• * * * * *. * * * *. * •• *. * *. * *. * * * * •• * * •• *** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95453 SOURCE, GA PACIFIC CORP HDWD STATION ID, 101-SD •• CASE NO.: 23679 SAMPLE TYPE, SOIL SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NO., KA94 BY, D RUMFORD ST, NC 1020 STOP, 00/00/00 ** •• ** ** ** *** * * * *. * * * * * ••• * * •• *. * * * * * *. * * * * * * * * * *. * * * * •• * * * * * * *. * * * •• * * * *. * *** UG/KG 720U 720U 720U 720U 720U 720U 720U 720U 720U 720U 720U 720U 720U 720U 720U 720U 720U 720U 720U 720U 720U 720U 720U 720U 720U 1B00U 720U 1800U . 720U 720U 720U ANALYTICAL RESULTS PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLCROBENZENE 1,4-DICHLCROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL 2,2'-CHLOROISOPROPYLETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY) METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLCROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLCPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLCROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE ***FOOTNOTES*** UG/KG 1800U 720U 1800U 1800U 720U 720U 720U 720U 720U 1800U 1B00U 720U 720U 720U 1800U 720U 720U 720U 720U 110J 140J 720U 720U 720U 720U 720U 720U 110J 720U 720U 720U 720UJ 54 ANALYTICAL RESULTS 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLCROBENZENE (HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHI)PERYLENE PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC.INDICATES THAT DATA·UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. == llliiliiil liiliiii iilil ---- -------__ : EXTRACTABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. OB/15/95 *** * * ••• * •• * * *. * •• * * * * * * *. * * * *. * * * * * * * * * * * * * *. * * *. * * *. * * * * * * * •••• *** •• ** ** •• PROJECT NO. 95-0293 SAMPLE NO. 95454 SOURCE, GA PACIFIC CORP HDWD STATION ID, 004-SL ~ ** CASE NO.: 23679 SAMPLE TYPE, SOIL SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NO., KA95 BY, D RUMFORD ST, NC 1125 STOP, 00/00/00 •• ** ** ** ** ***. * * * * * * •• * * * * * * * *. * * * * * * * * * * * * * * * *. * * * * *. * * ••• * *. * * * * * * * * *. * * * *** UG/KG 1ioou 12000 12000 12000 1200U 1200U 12000 12000 1200U 12000 12000 1200U 12000 1200U 1200U 12000 12000 12000 12000 12000 12000 12000 12000 12000 12000 31000 12000 31000 12000 12000· 12000 ANALYTICAL RESULTS PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL 2,2'-CHLOROISOPROPYLETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY) METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE ***FOOTNOTES*** UG/KG 31000 12000 31000 31000 1200U 1200U 12000 1200U 12000 31000 31000 12000 12000 12000 6900 12000 1200U 12000 12000 12000 1200UJ 12000 12000 1200U 12000 12000 12000 12000 12000 12000 1200U 1200UJ 20 ANALYTICAL RESULTS 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE. 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE . BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHI)PERYLENE PERCENT MOISTURE *A-AVERAGE VALUE . *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. !!!!I == liiiii liiiil .. --- ------ --- EXTRACTABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** •••••• * * •• * * •••••• * * •• * * * * * *. * * •• * * * *. *. *. *. * *. * * * * *. * * *. * •• * * ••• ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95455 SOURCE: GA PACIFIC CORP HDWD STATION ID: 002-SL ** CASE NO.: 23679 SAMPLE TYPE: SOIL SAS NO.: PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/20/95 D. NO.: KAA96 BY: D RUMFORD ST: NC 1155 STOP: 00/00/00 ** ** ** ** ** *** * •••• * •• * * •• * * ••• * * * * * * * * *. * *. *. * * * * *. * *. * •• * ••• * *. *. * *. *. * * * * *** UG/KG 570U 570U 570U 570U 570U 570U 570U 570U 570U 570U 570U 570U 570U 570U 570U 570U 570U 570U 570U 570U 570U 570U 570U 570U 570U 1400U 570U 1400U 570U 570U 570U ANALYTICAL RESULTS PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL 2,2'-CHLOROISOPROPYLETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISO PHO RONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY) METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE ***FOOTNOTES*** UG/KG 1400U 570U 1400U 1400U 570U 570U 570U 570U 570U 1400U 1400U 570U 570U 570U 1400U 570U 570U 570U 570U 120J 190J 570U 570U 570U 120J 570U 570U 260J 76J 570U 570U 570UJ 42 ANALYTICAL RESULTS 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE ' CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHI)PERYLENE PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED. *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. !!!!!I Iii& iili iiiil -- --- -- -- - ---- EXTRACTABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, 'GA. 08/15/95 *** * *. * * * * * * * •• * *. * *. * * * * * * * *. * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * *. * *** •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95456 SOURCE: GA PACIFIC CORP HDWD STATION ID: 009-SW' ** CASE NO.: 23679 SAMPLE TYPE: SURFACEWA SAS NO.: PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/19/95 D.NO.:KA79 BY: D RUMFORD ST: NC 1350 STOP: 00/00/00 •• •• • • •• •• ***. * * * * * •• * *. * * *. *. * * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * *·* * * * *** UG/L 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U. 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 25U 10U 25U 10U 10U 10U ANALYTICAL RESULTS PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL 2,2'-CHLOROISOPROPYLETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISO PHO RONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY) METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE ***FOOTNOTES*** UG/L 25U lOU 25U 25U lOU lOU lOU lOU lOU 25U 25U lOU lOU lOU 2SU lOU lOU lOU lOU lOU lOUJ lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOUJ ANALYTICAL RESULTS 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHI)PERYLENE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. liiiil liiEI --- --- -- ------' '; EXTRACTABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 ***. * * * * * *. * * * * * *. * * * * * * * * * * •• *. * * * * * * * * * * * * * * * * * * * * * •• * *. * * *. * •• *** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95457 SOURCE, GA PACIFIC CORP HOWD STATION ID, 009-SD, ** CASE NO.: 23679 SAMPLE TYPE, SOIL SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 D. NO., KABO BY, D RUMFORD ST, NC 1425 STOP, 00/00/00 ** ** ** ** ** *** * * * *. * * * * * •• * *. * * * * * *. * *. * *. * •• * * •• * *. * * * * * * * *. *. *. * * * * * * *. * *. *** UG/KG 810U 810U 810U 810U 810U 810U 810U 810U 1200 810U 810U 810U 810U 810U 810U 810U 810U 810U 810U 810U 810U 810U 810U 810U 810U 2000U 810U 2000U 810U 810U 810U ANALYTICAL RESULTS PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL 2,2'-CHLOROISOPROPYLETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY) METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE ***FOOTNOTES*** UG/KG 2000U BlOU 2000U 2000U BlOU BlOU BlOU BlOU 810U 2000U 2000U 810U 810U 810U 9500 200J 810U 810U 810U 420J 810J 810U 810U 810U 490J 810U 810U 870 460J 230J 810U 260J 60 ANALYTICAL RESULTS 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHI)PERYLENE PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAT-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE .OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER rs THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS rs NECESSARY FOR VERIFICATION. .. ------111!!!!!!1 l!!!!!I --iliil - EXTRACTABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95458 SOURCE, GA PACIFIC CORP HDWD STATION ID, 010-SW / ** CASE NO.: 23679 SAMPLE TYPE, SURFACEWA SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 D. NO., KA81 BY, D RUMFORD ST, NC 1615 STOP, 00/00/00 ** ** ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L ANALYTICAL RESULTS lOU PHENOL lOU BIS(2-CHLOROETHYL) ETHER lOU 2-CHLOROPHENOL lOU 1,3-DICHLOROBENZENE lOU 1,4-DICHLOROBENZENE lOU 1,2-DICHLOROBENZENE lOU 2-METHYLPHENOL lOU 2,2'-CHLOROISOPROPYLETHER lOU (3-AND/OR 4-)METHYLPHENOL lOU N-NITROSODI-N-PROPYLAMINE lOU HEXACHLOROETHANE lOU NITROBENZENE lOU ISOPHORONE lOU 2-NITROPHENOL lOU 2,4-DIMETHYLPHENOL lOU BIS(2-CHLOROETHOXY) METHANE lOU 2,4-DICHLOROPHENOL lOU 1,2,4-TRICHLOROBENZENE lOU NAPHTHALENE lOU 4-CHLOROANILINE lOU HEXACHLOROBUTADIENE lOU 4-CHLOR0-3-METHYLPHENOL lOU 2-METHYLNAPHTHALENE lOU HEXACHLOROCYCLOPENTADIENE (HCCP) lOU 2,4,6-TRICHLOROPHENOL 25U 2,4,5-TRICHLOROPHENOL lOU 2-CHLORONAPHTHALENE 25U 2-NITROANILINE lOU DIMETHYL PHTHALATE lOU ACENAPHTHYLENE lOU 2,6-DINITROTOLUENE ***FOOTNOTES*** UG/L 25U lOU 25U 25U lOU lOU lOU lOU lOU 25U 25U lOU lOU lOU 25U lOU lOU lOU lOU lOU lOUJ lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOUJ ANALYTICAL RESULTS 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHI)PERYLENE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC.INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -... -I!!!!!!!!! - ----- -- EXTRACTABLE ORGANICS DATA REPORT ••••• •-· * •• *. * * * * * ••• * * * •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95459 SOURCE: GA PACIFIC CORP HDWD STATION ID: 010-SD ** CASE NO.: 23679 SAMPLE AND ANALYSIS-MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 •• * * * * * ••• * *. * * * * * * * * * * * * * * * * *. * *. * * * * * * * * *** SAMPLE TYPE: SOIL SAS NO.: PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/19/95 D. NO.: KA82 BY: D RUMFORD ST: NC 1620 STOP: 00/00/00 •• •• • • •• •• *** * *. * * * *. *. * * *. * * * * * * * * * * * * * * * * * •• * * *. * * *. * *. * * * * * * * * * *. * * *. * * * ••• UG/KG 620U 620U 620U 620U 620U 620U 620U 620U 620U 620U 620U 620U 620U 620U 620U 620U 620U 620U 620U 620U 620U 620U 620U 620U 620U 1600U 620U 1600U 620U 620U 620U ANALYTICAL RESULTS PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL 2,2'-CHLOROISOPROPYLETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY) METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE ***FOOTNOTES*** UG/KG 1600U 620U 1600U 1600U 620U 620U 620U 620U 620U 1600U 1600U 620U 620U 620U 1600U 620U 620U 620U 620U 120J 150J 620U 620U 620U 620U 620U 620U 120J 620U 620U 620U 620UJ 47 ANALYTICAL RESULTS 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE . BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHI)PERYLENE PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE .EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. - ----l!!!!!!I liiiiilil iilil -- ---- SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. REPRINTED ON 08/21/95 EXTRACTABLE ORGANICS DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95460 SOURCE, GA PACIFIC CORP HDWD STATION ID, 109-SW ** CASE NO.: 23679 SAMPLE TYPE, SURFACWA SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 D. NO., KA83 BY, D RUMFORD ST, NC 1350 STOP, 00/00/00 •• •• • • •• •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L lOU 10U lOU 10U lOU 10U lOU lOU lOU lOU lOU 10U lOU lOU lOU lOU lOU lOU 10U 10U lOU lOU lOU lOU lOU 25U lOU 25U lOU lOU lOU ANALYTICAL RESULTS PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL 2,2'-CHLOROISOPROPYLETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY) METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE ***REMARKS*** ***FOOTNOTES*** UG/L 25U lOU 25U 25U lOU 10U lOU lOU lOU 25U 25U lOU lOU lOU 25U 10U 10U 10U lOU 10U lOUJ 10U ·1ou lOU 10U 10U lOU lOU lOU 10U lOU lOUJ ANALYTICAL RESULTS 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHI)PERYLENE ***REMARKS*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER rs THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS rs NECESSARY FOR VERIFICATION. ----liiliil liiil ------- - EXTRACTABLE ORGANICS DATA REPORT · SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * * ·• * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95461 SOURCE, GA PACIFIC CORP HDWD STATION ID, 109-SD ** CASE NO.: 23679 SAMPLE TYPE, SOIL SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 D. NO., KA84 BY, D RUMFORD ST, NC 1425 STOP, 00/00/00 •• •• • • •• •• *** * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG 2400U 2400U 2400U 2400U 2400U 2400U 2400U 2400U 2400U 2400U 2400U 2400U 2400U 2400U 2400U 2400U 2400U 2400U 2400U 2400U 2400U 2400U 2400U 2400U 2400U 6000U 2400U 6000U 2400U 2400U 2400U ANALYTICAL RESULTS PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL 2,2'-CHLOROISOPROPYLETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY) METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE ***FOOTNOTES*** UG/KG 6000U 2400U 6000U 6000U 2400U 2400U 2400U 2400U 2400U 6000U 6000U 2400U 2400U 2400U 9200 2400U 2400U 2400U 2400U 410J 640J 2400U 2400U 2400U 410J 2400U 2400U 680J 340J 2400U 2400U 2400UJ 59 ANALYTICAL RESULTS 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE '1, 3' -DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHI)PERYLENE PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -·-- - - 1!!11!1 == == liiliiil liiiil - -- -- - EXTRACTABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95462 SOURCE, GA PACIFIC CORP HDWD STATION ID, 013-RN ** CASE NO.: 23679 SAMPLE TYPE, SURFACWA SAS NO., FROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 D. NO., KA97 BY, D RUMFORD ST, NC 0700 STOP, 00/00/00 •• •• • • •• •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU 25U lOU 25U lOU lOU lOU ANALYTICAL RESULTS PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 2-METHYLPHENOL 2,2'-CHLOROISOPROPYLETHER (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY) METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4 -CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE ACENAPHTHYLENE 2,6-DINITROTOLUENE ***FOOTNOTES*** UG/L 25U lOU 25U 25U lOU lOU lOU lOU lOU 25U 25U lOU lOU lOU 25U lOU lOU lOU lOU lOU lOUJ lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOUJ ANALYTICAL RESULTS 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL NcNITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHI)PERYLENE . *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT.' RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -----1!!!111 l!!!!l!I == lilliii ----- - - SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT 08/15/95 *** *. *. * * * ••• *. * * *. * * *. * * * *. * * *. * * * *. * *. * * *. * * * * * * *. *. * * *. * *. * * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE-NO. 95445 SOURCE, GA PACIFIC CORP HDWD SAMPLE TYPE, SOIL STATION ID, 007-SL CASE.NO., 23679 SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NO., KA86 BY, D RUMFORD ST, NC 0900 STOP, 00/00/00 MD NO, KA86 •• •• •• •• •• *** * * * * * * * * *. * * •• * * * * * * * * *. * * * * •• * * *. * * * * * * * * * * * * * * * *. * * * * *. * •• * * *** ***REMARKS*** EXCESSIVE HOLDING TIME *.**FOOTNOTES*** 50000JN BOOOOJN 40000JN 60000JN lOOOOJN 20000JN lOOOOOJN 300000JN 200000JN" lOOOOOJN 400000J ANALYTICAL RESULTS UG/KG TETRACHLOROPHENOL DIMETHYLPHENANTHRENE (3 ISOMERS) TRIMETHYLPHENANTHRENE (2 ISOMERS) METHYLPYRENE (2 ISOMERS) BENZANTHRACENONE TETRACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN (2 ISOMERS) TETRACHLOROBENZENE (2 ISOMERS) HEXACHLORODIBENZODIOXIN OCTACHLORODIBENZODIOXIN 6 UNIDENTIFIED COMPOUNDS ***REMARKS*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT.NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. ----I!!!!! liiiiii liiii -- -- - - -- SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT 08/15/95 *** * * ••• * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * + * * * *** ** ** ** .** ** PROJECT NO. 95-0293 SAMPLE NO. 95446 SOURCE: GA PACIFIC CORP HDWD STATION ID: 107-SL CASE.NO.: 23679 SAS NO.: SAMPLE TYPE: SOIL PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/20/95 D. NO.: KA87 BY: D RUMFORD ST: NC 0900 STOP: 00/00/00 MD NO: KA87 ** ** ** ** ** *** * * * * * •• *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * *** ***REMARKS*** EXCESSIVE HOLDING TIME 3+E06JN 500000J ANALYTICAL RESULTS UG/KG TETRACHLOROPHENOL 11 UNIDENTIFIED COMPOUNDS ***REMARKS*** ***FOOTNOTES*** *A-AVERAGE VALUE ·•NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -·-.. -l!!!l!!!!!!I 1!!11!!1 I!!!!!! iliiii iiliiil illlii - - - SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT 08/15/95 *** * * * * *·* * *. * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95447 SOURCE, GA PACIFIC CORP HDWD STATION ID, 003-SL CASE.NO., 23679 SAS NO., SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NO., KABB BY, D RUMFORD ST, NC 0950 STOP, 00/00/00 MD NO, KABB •• •• •• •• •• *** * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ***FOOTNOTES*** 300JN 3000J ANALYTICAL RESULTS UG/KG TETRACHLOROPHENOL 4 UNIDENTIFIED.COMPOUNDS *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION . ---- - .. -- - ----.. SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT 08/15/95 ***. * * * * ••• *. * * * •• * * * •• * * * * * * * * * * *. * * * * * * * * * * * •• * * * * •• * * * * * * * *. * * *** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95448 SOURCE, GA PACIFIC CORP HDWD STATION ID, 005-SL CASE.NO., 23679 SAS NO., SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NO., KA89 BY, D RUMFORD ST, NC 1020 STOP, 00/00/00 MD NO, KA89 ** ** •• ** ** *** *. * * * * •• * * * •• * *. * * * *. *. *. * •• * * *. * •. * •• * * *. * * * * * * * *. *. * * * * * * •• * * *** ***FOOTNOTES*** 900JN 70000J ANALYTICAL RESULTS UG/KG HEXACHLOROBIPHENYL 28 UNIDENTIFIED COMPOUNDS *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE. IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN . *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. liiil - --- --- SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, ,GA. MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT 08/15/95 *** * * * *. * * * * * * * * * * * *. * * * * * * * * * *. * * * * * ·* * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95451 SOURCE, GA PACIFIC CORP HDWD STATION ID, 001-SD CASE.NO., 23679 SAS NO., SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NO., KA92 BY, D RUMFORD ST, NC 1020 STOP, 00/00/00 MD NO, KA92 •• •• • • •• •• *** * * *. * * * * * * * * * * * * * •• *. * * * * * * * * * * * * * * *. * * * * *. * * * * * * * * * * * * *. * * * * * *** ***FOOTNOTES*** BOOJN 3000J ANALYTICAL RESULTS UG/KG TETRACHLOROPHENOL 2 UNIDENTIFIED COMPOUNDS *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. ~11111!11.:,__ ______ .. 1!!!!!!1--m=-==-· --. -- - -- -- ---- SAMPLE AND ANALYSIS·MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT 08/15/95 *** * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE·NO. 95453 SOURCE: GA PACIFIC CORP HDWD STATION ID: 101-SD CASE.NO.: 23679 SAS NO.: SAMPLE TYPE: SOIL PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/20/95 D. NO.: KA94 BY: D RUMFORD ST: NC 1020 -STOP: 00/00/0~ MD NO: KA94 ** ** ** ** ** *** * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** 7000J ***FOOTNOTES*** ANALYTICAL RESULTS UG/KG 4 UNIDENTIFIED COMPOUNDS *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES ~J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. ----· -~--------==--iiii ----- -- -- SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT 08/15/95 *** •• *. * •••••• * * * * *. * *. * * * •• * * *. * * * * * * *. *-* *. * * * *. * •• *. * *. *. * * *. * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95454 SOURCE, GA PACIFIC CORP HDWD SAMPLE TYPE, SOIL STATION ID, 004-SL CASE.NO., 23679 SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NO., KA95 BY, D RUMFORD ST, NC 1125 STOP, 00/00/00 MD NO, KA95 •• •• •• •• •• *** *· * ••• * ••• * * * * •• *. * * *. * *. * ••• *. * * * * * * * * * *. * * * * * * * * * * *. * * *. * * * * * *** ***FOOTNOTES*** lOOOJN 9000J ANALYTICAL RESULTS UG/KG TETRACHLOROPHENOL 4 UNIDENTIFIED COMPOUNDS *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER rs THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS rs NECESSARY FOR VERIFICATION. -- - -- -- -- - SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT 08/15/95 *** * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95455 SOURCE, GA PACIFIC CORP HDWD STATION ID, 002-SL CASE.NO., 23679 SAS NO·., SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NO., KAA96 BY, D RUMFORD ST, NC 1155 STOP, 00/00/00 MD NO, KA96 •• •• •• •• •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** 9000J ***FOOTNOTES*** ANALYTICAL RESULTS UG/KG 10 UNIDENTIFIED COMPOUNDS *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. lililil liiilil -- - _, SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT 08/15/95 *** * * •• * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95457 SOURCE, GA PACIFIC CORP HDWD· SAMPLE TYPE, SOIL STATION ID, 009-SD CASE.NO., 23679 SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 D. NO., KAB0 BY, D RUMFORD ST, NC 1425 STOP, 00/00/00 MD NO, KAB0 •• •• •• •• •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ***FOOTNOTES*** 1000JN 20000J ANALYTICAL RESULTS UG/KG BENZENEACETIC ACID 15 UNIDENTIFIED COMPOUNDS *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. _--------------------1!!!!9-: ==------iiiii ---- SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT 08/15/95 *** * * *. * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95459 SOURCE: GA PACIFIC CORP HDWD SAMPLE TYPE: SOIL STATION ID: 010-SD CASE .NO.: 23679 SAS NO.: PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/19/95 D. NO.: KA82 BY: D RUMFORD ST: NC 1620 STOP: 00/00/00 MD NO: KA82 •• •• •• •• •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** 5000J ***FOOTNOTES*** ANALYTICAL RESULTS UG/KG 6 UNIDENTIFIED COMPOUNDS *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE .GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -·-••-----· ----------1!!!!!!!!1-· l!!!!!!!!l-l!!!!l!!l-1!1!111-· --!!!!!!1-!!!!!!I~-------:-· SAMPLE AND ANALYSIS MANAGEMENT-SYSTEM EPA-REGION IV ESD, ATHENS, GA. MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT 08/15/95 *** * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95461 SOURCE, GA PACIFIC CORP HDWD SAMPLE TYPE, SOIL STATION ID, 109-SD CASE.NO., 23679 SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 D. NO., KA84 BY, D RUMFORD ST, NC 1425 STOP, 00/00/00 MD NO, KA84 ** ** ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * *** lOOOOJ ***FOOTNOTES*** ANALYTICAL RESULTS UG/KG 3 UNIDENTIFIED COMPOUNDS *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE. *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES.THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -· --· 11!!!!!!1-11!1!!!1-· --· 1!!1!!1---liiillil iiii liiliil - ----- --- I -I I I . I I I I UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region IV Environmental Services Division College Station Road, Athens, Ga. 30613 g.***MEMORANDUM*****~ I n DATE: 08/16/95 ' SUBJECT: n •. FROM: Results 95-0293 of 1 Pesticide/PCB Analysis; GA PACIFIC CORP HDWD PLYMOUTH NC I{ _;?,,SE N~: 23679 arles H.· ~fv hief, Laboratory Evaluation/Quality Assurance Section TO: PAT DEROSA I I Attached are the results of analysis of samples collected as part of fie subject project. AJ a result of the Quality Assurance Review, certain data qualifiers ir'.Y have been placed on the data. Attached is a DATA QUALIFIER rPORT which explains, the reasons that these qualifiers were required. I If you have any questions please contact me. 1: . 1: I I: I I I ATTACHMENT I d D • I I: I 1: ' I! I I: I I I I, I I I I I ORGANIC DATA QUALIFIER REPORT Case Number 23679 Project Number 95-0293 Site ID.' Georgia Pacific Corp HDIJD, Plymouth, NC SAS Number Affected Sampl:es Volatiles all samples 95446 95447,95453, 95455 Extractables ~o~ 95445,95446 95447,95450, 95452,95454, 95456,95458, 95460,95462 95448 95451 95453,95455, 95459 95455 95457 95461 Compound or Fraction chloromethane benzene toluene chlorobenzene 2-butanone all compounds pyrene benzo(g,h,i)perylene pyrene di-n-octylphthalate benzo(b/k)fluoranthene benzo(a)pyrene indeno(l,2,3-cd)pyrene dibenz(a,h)anthracene benzo(g,h,i)perylene pyrene . benzo(b/k)fluoranthene benzo(g,h,i)perylene fluoranthene pyrene benzo(b/k)fluoranthene benzo(g,h,i)perylene benzo(a)pyrene chrysene phenanthrene fluoranthene pyrene chrysene benzo(a)pyrene indeno(l,2,3-cd)pyrene benzo(g,h,i)perylene fluoranthene pyrene chrysene benzo(b/k)fluoranthene benzo(a)pyrene benzo(g,h,i)perylene R J J J J J J J J J J J J J J J J J J J J J J J J J J J J J J J J J J J J Flag Used Reason unacceptable PE sample recovery < quantitation limit < quantitation limit < quantitation limit < quantitation limit exceeded extraction holding time low PE sample recovery low PE sample recovery low PE sample recovery low internal standard recovery low internal standard recovery low internal standard recovery low internal standard recovery low internal standard recovery low internal standard recovery < quantitation limit < quantitation limit low PE sample recovery < quantitation limit < quantitation limit < quantitation limit low PE sample recovery < quan ti ta tion limit < quantitation limit < quantitation limit < qunatitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit low PE sample recovery I I I ' I I I I I I oc> I 0"" ' I I I I ' I I I :1 I I II ;I ,1 :I ' ORGANIC DATA QUALIFIER REPORT Case Number 23679 Affected Samples Compound or Fraction Pesticides all samples 95445,95446 95447 95454 95455 95457 95459 aroclor-1016 alpha-bhc delta-bhc gamma-bhc 4,4'-DDE 4,4'-DDT beta-bhc 4,4' -ODE delta-bhc gamma-bhc endrin aldehyde 4,4'-DDE Project Number 95-0293 Flag Used R C C C J J J J J N J J J N Reason unacceptable PE sample recovery GC/MS confirmed GC/MS confirmed GC/MS confirmed < quantitation limit < quantitation limit < qua!}titation limit < quantitation limit < quantitation limit difference in column quantitations < quantitation limit < quantitation limit < quantitation limit difference in column quantitations PESTICIDES/PCB'S DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95445 SOURCE, GA PACIFIC CORP HDWD STATION ID, 007-SL / CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NUMBER, KA86 BY, D RUMFORD ST, NC 0900 STOP, 00/00/00 •• •• •• •• • • *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS 31000C ALPHA-BHC 8300U METHOXYCHLOR 12000U BETA-BHC 1600U ENDRIN KETONE 48000C DELTA-BHC 1600U ENDRIN ALDEHYDE 72000C GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 830U HEPTACHLOR .830U GAMMA-CHLORDANE /2 830U ALDRIN 830U ALPHA-CHLORDANE /2 830U HEPTACHLOR EPOXIDE 83000U TOXAPHENE 830U ENDOSULFAN I (ALPHA) 16000UR PCB-1016 (AROCLOR 1016) 1600U DIELDRIN 33000U PCB-1221 (AROCLOR 1221) 1600U 4,4' -ODE (P, P' -DDE) 16000U PCB-1232 (AROCLOR 1232) 1600U ENDRIN 16000U PCB-1242 (AROCLOR 1242) 1600U ENDOSULFAN II (BETA) 16000U PCB-1248 (AROCLOR 1248) 1600U 4,4' -DOD (P, P' -DOD) 16000U PCB-1254 (AROCLOR 1254) 1600U ENDOSULFAN SULFATE 16000U PCB-1260 (AROCLOR 1260) 1600U 4,4'-DDT (P,P'-DDT) 59 PERCENT MOISTURE ***REMARKS*** ***REMARKS••~ ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF.PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT .. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. *C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE. ---==---liiiiil iiil ---- -- -- -- ---- PESTICIDES/PCB'S DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95446 SOURCE, GA PACIFIC CORP HDWD STATION ID, 107-SL ✓ CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NUMBER, KA87 BY, D RUMFORD ST, NC 0900 STOP, 00/00/00 *** * * * * * * * * * * * * * * * * * * * * * * * * ·* * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS 55000C ALPHA-BHC 9200U METHOXYCHLOR 3600U BETA-BHC 1800U ENDRIN KETONE 00000c DELTA-BHC 1800U ENDRIN ALDEHYDE 130000C GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 920U HEPTACHLOR 920U GAMMA-CHLORDANE /2 920U ALDRIN 920U ALPHA-CHLORDANE /2 920U HEPTACHLOR EPOXIDE 92000U TOXAPHENE 920U ENDOSULFAN I (ALPHA) 18000UR PCB-1016 (AROCLOR 1016) 1800U DIELDRIN 36000U PCB-1221 (AROCLOR 1221) 1800U 4,4'-DDE (P,P' -DOE) 18000U PCB-1232 (AROCLOR 1232). 1800U ENDRIN 18000U PCB-1242 (AROCLOR 1242) 1800U ENDOSULFAN II (BETA) 18000U PCB-1248 (AROCLOR 1248) 1800U 4,4' -ODD (P, P' -DOD) 18000U PCB-1254 (AROCLOR 1254) 1800U ENDOSULFAN SULFATE 18000U PCB-1260 (AROCLOR 1260) 1800U 4,4' -DDT (P, P' -DDT) 63 PERCENT MOISTURE ***REMARKS*** ***REMARKS*** ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER rs THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. *C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE. liiiil - ---- - -- - --- PESTICIDES/PCB'S DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• • • •• •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95447 SOURCE, GA PACIFIC CORP HDWD· STATION ID, 003-SL ✓ CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NUMBER, KA88 BY, D RUMFORD ST, NC 0950 STOP, 00/00/00 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS 2.2U ALPHA-BHC 22U METHOXYCHLOR 2.2U BETA-BHC 4 .2U ENDRIN KETONE 2.2U DELTA-BHC 4.2U ENDRIN ALDEHYDE 2.2U GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 2.2U HEPTACHLOR 2.2U GAMMA-CHLORDANE /2 2.2U ALDRIN 2.2U ALPHA-CHLORDANE /2 2.2U HEPTACHLOR EPOXIDE 220U TOXAPHENE 2.2U ENDOSULFAN I (ALPHA) 42UR PCB-1016 (AROCLOR 1016) 4 .2U · DIELDRIN 85U PCB-1221 (AROCLOR 1221) 1. 7J 4,4'-DDE (P,P'-DDE) 42U PCB-1232 (AROCLOR 1232) 4 .2U ENDRIN 42U PCB-1242 (AROCLOR 1242) 4 .2U ENDOSULFAN II (BETA) 42U PCB-1248 (AROCLOR 1248) 4 .2U 4,4' -ODD (P, P' -ODD) 42U PCB-1254 (AROCLOR 1254) 4 .2U ENDOSULFAN SULFATE 42U PCB-1260 (AROCLOR 1260) l.9J 4,4' -DDT (P,P'-DDT) 21 PERCENT MOISTURE ***REMARKS*** ***REMARKS*** ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. *C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE. liilii iilii ---- --- -- - --- PESTICIDES/PCB'S DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. *** * * •• * *. * * * * * •• * * * * * * * * * *. * * * * * * * * * *·*. * * * * * ••••••• *. * * * * * * * ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95448 SOURCE: GA PACIFIC CORP HDWD STATION ID: 005-SL CASE NUMBER: 23679 SAS NUMBER: SAMPLE TYPE: SOIL FROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/20/95 D. NUMBER: KA89 BY: D RUMFORD ST: NC 1020 STOP: 00/00/00 08/15/95 • * * * *** ** ** ** ** ** ***. * * * * * ••• * •• * * * * * * * * *. * *. * * * * * *. * * •• *. * •• *. * * * *. * * •• * * * * * •••• * *** UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS 14U ALPHA-BHC 140U METHOXYCHLOR 14U BETA-BHC 27U ENDRIN KETONE 14U DELTA-BHC 27U ENDRIN ALDEHYDE 14U GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 14U. HEPTACHLOR 14U GAMMA-CHLORDANE /2 14U ALDRIN 15 ALPHA-CHLORDANE /2 14U HEPTACHLOR EPOXIDE 1400U TOXAPHENE 14U ENDOSULFAN I (ALPHA) 270UR PCB-1016 (AROCLOR 1016) 27U DIELDRIN 550U PCB-1221 (AROCLOR 1221) 27U 4,4'-DDE (P, P' -DOE) 270U PCB-1232 (AROCLOR 1232) 27U ENDRIN 270U PCB-1242 (AROCLOR 1242) 27U ENDOSULFAN II (BETA) 270U PCB-1248 (AROCLOR 1248) 27U 4, 4' -ODD (P, P' -DOD) 270U PCB-1254 (AROCLOR 1254) 27U ENDOSULFAN SULFATE 270U PCB-1260 (AROCLOR 1260) 27U 4,4'-DDT (P, P' -DDT) 40 PERCENT MOISTURE ***REMARKS*** ***REMARKS*** ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. *C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2 .. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE. -----·-- -- - --- SAMPLE AND ANALYSIS· MANAGEMENT SYSTEM PESTICIDES/PCB'S DATA REPORT EPA-REGION IV ESD, ATHENS, GA. 08/15/95 ***. * *. * ••• * ••• * * ••• * * * * * * •• * * *. * * * * * * * * * * * * * ••• * * *. * * * * * * * * * * *. * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95449 SOURCE, GA PACIFIC CORP HDWD STATION ID, 006-SL / CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NUMBER, KA90 BY, D RUMFORD ST, NC 1040 STOP, 00/00/00 ** •• •• • • •• *** ••••• *. * *. * * *. * * *. * * * * * *. *. * * * * * * * * * * * •• * * * * * * *. * * * * * •• * * *. *. * *** UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS NA ALPHA-BHC NA METHOXYCHLOR NA BETA-BHC NA ENDRIN KETONE NA DELTA-BHC NA ENDRIN ALDEHYDE NA GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 NA HEPTACHLOR NA GAMMA-CHLORDANE /2 NA ALDRIN NA ALPHA-CHLORDANE /2 NA HEPTACHLOR EPOXIDE NA TOXAPHENE NA ENDOSULFAN I (ALPHA) NA PCB-1016 (AROCLOR 1016) NA DIELDRIN NA PCB-1221 (AROCLOR 1221) NA 4,4'-DDE (P, P' -DOE) NA PCB-1232 (AROCLOR 1232) NA ENDRIN NA PCB-1242 (AROCLOR 1242) NA ENDOSULFAN II (BETA) NA PCB-1248 (AROCLOR 1248) NA 4,4' -DOD (P,P'-DDD) NA PCB-1254 (AROCLOR 1254) NA ENDOSULFAN SULFATE NA PCB-1260 (AROCLOR 1260) NA 4,4'-DDT (P, P' -DDT) PERCENT MOISTURE ***REMARKS*** ***REMARKS*** NO SAMPLE CONTAINER RECEIVED ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED .. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. *C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE. ----------· --- ------ SAMPLE AND ANALYSIS MANAGEMENT SYSTEM PESTICIDES/PCB'S DATA REPORT EPA-REGION IV ESD, ATHENS, GA. 08/15/95 ••• * * * *. * * * * * * * * * * •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95450 SOURCE, GA PACIFIC CORP HDWD STATION ID, 001-SW, CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, SURFACEWA PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NUMBER, KA91 BY, D RUMFORD ST, NC 1015 STOP, 00/00/00 •• •• •• • • •• *** * * * * * * * * * * ·• * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * *** UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS o.osou ALPHA-BHC a.sou METHOXYCHLOR o.osou BETA-BHC O.lOU ENDRIN KETONE o.osou DELTA-BHC O.lOU ENDRIN ALDEHYDE o.osou GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 o.osou HEPTACHLOR o.osou GAMMA-CHLORDANE /2 o.osou ALDRIN o.osou ALPHA-CHLORDANE /2 o.osou HEPTACHLOR EPOXIDE s.ou TOXAPHENE o.osou ENDOSULFAN I (ALPHA) 1.0UR PCB-1016 (AROCLOR 1016) O.lOU DIELDRIN 2.0U PCB-1221 (AROCLOR 1221) O.lOU 4,4'-DDE (P, P' -DDE) 1.0U PCB-1232 (AROCLOR 1232) O.lOU ENDRIN 1.0U PCB-1242 (AROCLOR 1242) O.lOU ENDOSULFAN II (BETA) 1.0U PCB-1248 (AROCLOR 1248) O.lOU 4, 4' -DOD (P, P' -DDD) 1.0U PCB-1254 (AROCLOR 1254) O.lOU ENDOSULFAN SULFATE 1.0U PCB-1260 (AROCLOR 1260) O.lOU 4,4'-DDT (P,P' -DDT) ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. --•C-CONFIRMED-BY-GGMS--------1.-WHEN-NO_VALUE_IS_REPORTED,_SEE~C~H=L=O=R~D~AN=E=-C=O=N=S=T=I.=T.=U.=Ec.NT=S'-'.'-----------------------2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE. --- - ----- ----- - --- SAMPLE AND ANALYSIS MANAGEMENT SYSTEM PESTICIDES/PCB'S DATA REPORT EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95451 SOURCE, GA PACIFIC CORP HDWD STATION ID, 001-SD, CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, SOIL FROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NUMBER, KA92 BY, D RUMFORD ST, NC 1020 STOP, 00/00/00 •• •• •• • • •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS 21U ALPHA-BHC 210U METHOXYCHLOR 21U BETA-BHC 41U ENDRIN KETONE 21U DELTA-BHC 41U ENDRIN ALDEHYDE 21U GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 21U HEPTACHLOR 21U GAMMA-CHLORDANE /2 21U ALDRIN 21U ALPHA-CHLORDANE /2 21U HEPTACHLOR EPOXIDE 2100U TOXAPHENE 21U ENDOSULFAN I (ALPHA) 410UR PCB-10t6 (AROCLOR 1016) 41U DIELDRIN 840U PCB-1221· (AROCLOR 1221) 41U 4,4'-DDE (P, P' -ODE) 410U PCB-1232 (AROCLOR 1232) 41U ENDRIN 410U PCB-1242 (AROCLOR 1242) 41U ENDOSULFAN II (BETA) 410U PCB-1248 (AROCLOR 1248) 41U 4,4' -DOD (P, P' -ODD) 410U PCB-1254 (AROCLOR 1254) 41U ENDOSULFAN SULFATE 410U PCB-1260 (AROCLOR 1260) 41U 4,4'-DDT (P,P'-DDT) 60 PERCENT MOISTURE ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. --.-*Ca.CONF.IRMED_B.Y GCMS . 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES-OF-TECHNICAL-CHLORDANE7.-----------------------------'-------------- -- ---- -- - - --- - PESTICIDES/PCB'S DATA REPORT *** * * •• * * * * * * * * * *. * * * * * •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95452 SOURCE: GA PACIFIC CORP HDWD STATION ID: 101-SW CASE NUMBER: 23679 SAS NUMBER: SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** SAMPLE TYPE: SURFACEWA PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/20/95 D. NUMBER: KA93 BY: D RUMFORD ST: NC 1015 STOP: 00/00/00 •• •• •• •• •• *** * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS o.osou ALPHA-BHC a.sou METHOXYCHLOR o.osou BETA-BHC O.lOU ENDRIN KETONE o.osou DELTA-BHC O.lOU ENDRIN ALDEHYDE o.osou GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 o.osou HEPTACHLOR o.osou GAMMA-CHLORDANE /2 o.osou ALDRIN o.osou ALPHA-CHLORDANE /2 o.osou HEPTACHLOR EPOXIDE 5.0U TOXAPHENE o.osou ENDOSULFAN I (ALPHA) 1.0UR PCB-1016 (AROCLOR 1016) O.lOU DIELDRIN ' 2.0U PCB-1221 (AROCLOR 1221) O.lOU 4, 4' -ODE (P, P' -DDE) l.OU PCB-1232 (AROCLOR 1232) O.lOU ENDRIN l.OU PCB-1242 (AROCLOR 1242) O.lOU ENDOSULFAN II (BETA) l.OU PCB-1248 (AROCLOR 1248) O.lOU 4,4' -DOD (P, P' -DDD) l.OU PCB-1254 (AROCLOR 1254) O.lOU ENDOSULFAN SULFATE l.OU PCB-1260 (AROCLOR 1260) O.lOU 4,4'-DDT (P,P'-DDT) ***FOOTNOTES*** *A-AVERAGE VALUE ·•NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. --•C-CONFl'RMED-BY-GCMS--------1-.-WHEN-NO_VALUE_IS_REPORTED,_SEE_CHLORDANE_CONSTITU~E~NT=S~-~----------------------2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE. .. . • -- ------------ ---,,,, ~ I PESTICIDES/PCB'S DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. *** •• *. * *. *. * •• * * *. * *. * * * *. * * * * •• * * * * * * * •• *. * *. * * * * * * * *. * * * * * * ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95453 SOURCE: GA PACIFIC CORP HDWD STATION ID: 101-SD..; CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE: SOIL PROG ELEM: NSF COLLECTED CITY, PLYMOUTH COLLECTION START: 06/20/95 D. NUMBER, KA94 BY, D RUMFORD ST, NC 1020 STOP: 00/00/00 08/15/95 *. * *** ** ** ** ** ** ***. * * ••••••••• * * * * •• * *. * * *. *. *. * * * * * * * * *. * *. *-* *. *. * * * * * * *. *. * * *. *** UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS 3.6U ALPHA-BHC 36U METHOXYCHLOR 3.6U BETA-BHC 7.lU ENDRIN KETONE 3.6U DELTA-BHC 7 .lU ENDRIN ALDEHYDE 3.6U GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 3.6U HEPTACHLOR 3.6U GAMMA-CHLORDANE /2 3 .6U ALDRIN 3 .6U ALPHA-CHLORDANE /2 3.6U HEPTACHLOR EPOXIDE 360U TOXAPHENE 3.6U ENDOSULFAN I (ALPHA) 71UR PCB-1016 (AROCLOR 1016) 7.lU DIELDRIN 1400 PCB-1221 (AROCLOR 1221) 7 .lU 4, 4' -DOE (P, P' -DDE) 71U PCB-1232 (AROCLOR 1232) 7.lU ENDRIN 71U PCB-1242 (AROCLOR 1242) 7.lU ENDOSULFAN II (BETA) 71U PCB-1248 (AROCLOR 1248) 7.lU 4, 4' -DOD (P, P' -ODD) 71U PCB-1254 (AROCLOR 1254) 7.lU ENDOSULFAN SULFATE 71U PCB-1260 (AROCLOR 1260) 7.lU 4,4' -DDT (P, P' -DDT) 54 PERCENT MOISTURE ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS.THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. *C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE. PESTICIDES/PCB'S DATA REPORT SAMPLE AND-ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * -* * .• * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95454 SOURCE: GA PACIFIC CORP HDWD SAMPLE TYPE: SOIL STATION ID: 004-SL - CASE NUMBER: 23679 SAS NUMBER: PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/20/95 D. NUMBER: KA95 BY: D RUMFORD ST: NC 1125 STOP: 00/00/00 *** * * * * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * ·* * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG •• •• •• •• • • ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS 11 ALPHA-BHC 110U METHOXYCHLOR 6.7J BETA-BHC 20U ENDRIN KETONE 11U DELTA-BHC 20U ENDRIN ALDEHYDE 21 GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 11U HEPTACHLOR 11U GAMMA-CHLORDANE /2 11U ALDRIN 11U ALPHA-CHLORDANE /2 11U HEPTACHLOR EPOXIDE 1100U TOXAPHENE 11U ENDOSULFAN I (ALPHA) 200UR PCB-1016 (AROCLOR 1016) 20U DIELDRIN 410U PCB-1221 (AROCLOR 1221) 20U 4,4' -ODE (P,P' -DOE) 200U PCB-1232 (AROCLOR 1232) 20U ENDRIN 200U PCB-1242 (AROCLOR 1242) 20U ENDOSULFAN II (BETA) 200U PCB-1248 (AROCLOR 1248) 20U 4,4' -DOD (P, P' -DOD) 600 PCB-1254 (AROCLOR 1254) 20U ENDOSULFAN SULFATE 200U PCB-1260 (AROCLOR 1260) 20U 4,4'-DDT (P,P' -DDT) 20 PERCENT MOISTURE ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT·DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. *C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE. PESTICIDES/PCB'S DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV.ESD, ATHENS, GA. 08/15/95 *** * *. * * *. * *. * * * * *. *. * *. * * * * * * *. * * * * *. * * •• * * * * * * * •• * *. * * * * •• * * * •• *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95455 SOURCE, GA PACIFIC CORP IIDWD STATION ID, 002-SL, CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NUMBER, KAA96 BY, D RUMFORD ST, NC 1155 STOP, 00/00/00 •• •• •• •• • • *** * * * * *. *. * * * * * * * * *. * •• * * * *. * * *. * *. * •• * * * * * *. *. * * * ••• * * * * * *. * * * * *** UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS .5 .5 ALPHA-BHC 29U METHOXYCHLOR 2.9U BETA-BHC 5.7U ENDRIN KETONE 8.6 DELTA-BHC 5.7U ENDRIN ALDEHYDE 12 GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 2.9U HEPTACHLOR 2.9U GAMMA-CHLORDANE /2 2.9U ALDRIN 2.9U ALPHA-CHLORDANE /2 2.9U HEPTACHLOR EPOXIDE 290U TOXAPHENE 2.9U ENDOSULFAN I (ALPHA) 57UR PCB-1016 (AROCLOR 1016) 5. 7U DIELDRIN 120U PCB-1221 (AROCLOR 1221) 3.5J 4, 4' -DOE (P, P' -DDE) 57U PCB-1232 (AROCLOR 1232) 5. 7U ENDRIN 57U PCB-1242 (AROCLOR 1242) 5. 7U ENDOSULFAN II (BETA) 57U PCB-1248 (AROCLOR 1248) 5. 7U 4,4'-DDD (P, P' -DDD) 57U PCB-1254 (AROCLOR 1254) 5.7U ENDOSULFAN SULFATE 57U PCB-1260 (AROCLOR 1260) 5.7U 4,4'-DDT (P, P' -DDT) 42 PERCENT MOISTURE ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. *C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE. PESTICIDES/PCB'S DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * •••• *. *. * *. * * * *. * * ••• *. *. * * * * •• *. *. * *. * ••• * *. * * * * * *. * *. *. * * *** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95456 SOURCE, GA PACIFIC CORP HDWD STATION ID, 009-SW _,. CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, SURFACEWA PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 D. NUMBER, KA79 BY, D RUMFORD ST, NC 1350 STOP, 00/00/00 ** ** ** ** ** ••• * * * * ••• * * * * * *. * * * •• * * * * ••• * *. * * * *. * * * * * * * * * * *. * * * * *. * * * * *. * *. * *** UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS o.osou ALPHA-BHC a.sou METHOXYCHLOR o.osou BETA-BHC 0.10U ENDRIN KETONE o.osou DELTA-BHC 0.10U ENDRIN ALDEHYDE o.osou GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 o.osou HEPTACHLOR o.osou GAMMA-CHLORDANE /2 o.osou ALDRIN o.osou ALPHA-CHLORDANE /2 o.osou HEPTACHLOR EPOXIDE 5.0U TOXAPHENE o.osou ENDOSULFAN I (ALPHA) 1.0UR PCB-1016 (AROCLOR 1016) 0.10U DIELDRIN 2.0U PCB-1221 (AROCLOR 1221) 0.10U 4, 4' -DOE (P,P'-DDE) 1.0U PCB-1232 (AROCLOR 1232) 0.10U ENDRIN 1.0U PCB-1242 (AROCLOR 1242) 0.10U ENDOSULFAN II (BETA) 1.0U PCB-1248 (AROCLOR 1248) 0.10U 4,4'-DDD (P, P' -DDD) 1.0U PCB-1254 (AROCLOR 1254) 0.10U ENDOSULFAN SULFATE 1.0U PCB-1260 (AROCLOR 1260) 0.10U 4,4'-DDT (P, P' -DDT) ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN . *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. *C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE. -- --·--- - iili liilla PESTICIDES/PCB'S DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95457 SOURCE, GA PACIFIC CORP HDWD STATION ID, 009-SD, CASE NUMBER,. 23679 SAS NUMBER, SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 D. NUMBER, KA80 BY, D RUMFORD ST, NC 1425 STOP, 00/00/00 08/15/95 * * * * *** •• •• •• •• *** * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS 21U ALPHA-BHC 210U METHOXYCHLOR 21U BETA-BHC 41U ENDRIN KETONE 3.7JN DELTA-BHC llJ ENDRIN ALDEHYDE 5 .3J GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 21U HEPTACHLOR 21U GAMMA-CHLORDANE /2 21U ALDRIN 21U ALPHA-CHLORDANE /2 21U HEPTACHLOR EPOXIDE 2100U TOXAPHENE 21U ENDOSULFAN I (ALPHA) 410UR PCB-1016 (AROCLOR 1016) 41U DIELDRIN 820U PCB-1221 (AROCLOR 1221) 41U 4, 4' -DOE (P, P' -ODE) 410U PCB-1232 (AROCLOR 1232) 41U ENDRIN 410U PCB-1242 (AROCLOR 1242) 41U ENDOSULFAN II (BETA) 410U PCB-1248 (AROCLOR 1248) 41U 4,4'-DDD (P, P' -DOD) 410U PCB-1254 (AROCLOR 1254) 41U ENDOSULFAN SULFATE 410U PCB-1260 (AROCLOR 1260) 41U 4,4'-DDT (P,P'-DDT) 60 PERCENT MOISTURE ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE. *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL. *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. *C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE. liilR liiiill PESTICIDES/PCB'S DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. *** •• * •• *. * ••• *. * * *. * *. * * * * * * * * •• * * * * * * * * * * *. *. * * * * * •• *. * * * * * ** •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95458 SOURCE: GA PACIFIC CORP HDWD STATION ID: 010-SW / CASE NUMBER: 23679 SAS NUMBER: SAMPLE TYPE: SURFACEWA PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/19/95 D. NUMBER: KA81 BY: D RUMFORD ST: NC 1615 STOP: 00/00/00 08/15/95 * * * * *** ** •• ** ** ** *** *. * •• * •• * •• * * •• * * * * * * * •• * * * * * * * * * *. *. * * ••• * * * * * * * * * *. * *. * * * *. * *** UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS 0.050U ALPHA-BHC 0.50U METHOXYCHLOR 0.050U BETA-BHC O.lOU ENDRIN KETONE 0.050U DELTA-BHC O.lOU ENDRIN ALDEHYDE 0.050U GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 0.050U HEPTACHLOR 0.050U GAMMA-CHLORDANE /2 0.050U ALDRIN 0.050U ALPHA-CHLORDANE /2 0.050U HEPTACHLOR EPOXIDE 5.0U TOXAPHENE 0.050U ENDOSULFAN I (ALPHA) l.OUR PCB-1016 (AROCLOR 1016) O.lOU DIELDRIN 2.0U PCB-1221 (AROCLOR 1221) O.lOU 4,4'-DDE. (P,P'-DDE) l.OU PCB-1232 (AROCLOR 1232) O.lOU ENDRIN l.OU PCB-1242 (AROCLOR 1242) O.lOU ENDOSULFAN II (BETA) l.OU PCB-1248 (AROCLOR 1248) O.lOU 4,4'-DDD (P,P'-DDD) l.OU PCB-1254 (AROCLOR 1254) O.lOU ENDOSULFAN SULFATE l.OU PCB-1260 (AROCLOR 1260) O.lOU 4,4' -DDT (P, P' -DDT) ***FOOTNOTES*** *A-AVERAGE VALUE· *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. *C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE. (--·-- ---.. iiil ra;;a PESTICIDES/PCB'S DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * *. * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** •• ** •• •• PROJECT NO. 95-0293 SAMPLE NO. 95459 SOURCE, GA PACIFIC CORP HDWD STATION ID, 010-SD / CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 D. NUMBER, KA82 BY, D RUMFORD ST, NC 1620 STOP, 00/00/00 •• •• •• •• ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS 16U ALPHA-BHC 160U METHOXYCHLOR 16U BETA-BHC 31U ENDRIN KETONE 16U DELTA-BHC 31U ENDRIN ALDEHYDE 16U GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 16U HEPTACHLOR 16U GAMMA-CHLORDANE /2 16U ALDRIN 16U ALPHA-CHLORDANE /2 16U HEPTACHLOR EPOXIDE 1600U TOXAPHENE 16U ENDOSULFAN I (ALPHA) 310UR PCB-1016 (AROCLOR 1016) 31U DIELDRIN 630U PCB-1221 (AROCLOR 1221) 3.0JN 4,4' -DOE (P,P'-DDE) 310U PCB-1232 (AROCLOR 1232) 31U ENDRIN 310U PCB-1242 (AROCLOR 1242) 31U ENDOSULFAN II (BETA) 310U PCB-1248 (AROCLOR 1248) 31U 4,4' -DOD (P, P' -DOD) 310U PCB-1254 (AROCLOR 1254) 31U ENDOSULFAN SULFATE 310U PCB-1260 (AROCLOR 1260) 31U 4,4' -DDT (P, P' -DDT) 47 PERCENT MOISTURE ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J~ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN .•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. *C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE. ' ~ ' - - -- ---iiii, lillil iiillil ==-------· 1!1!!!1----J!ll!lt ' PESTICIDES/PCB'S DATA REPORT *** * * * * * *. * * * * * * *. *. * * * * * SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ** ** ** ** •• PROJECT NO. 95-0293 SAMPLE NO. 95460 SOURCE, GA PACIFIC CORP HDWD SAMPLE TYPE, SURFACWA PROG ELEM, NSF COLLECTED CITY, PLYMOUTH BY, D RUMFORD ST, NC STATION ID, 109-SW ✓ CASE NUMBER, 23679 SAS NUMBER, COLLECTION START, 06/19/95 D. NUMBER, KA83 1350 STOP, 00/00/00 08/15/95 * * * * *** ** •• ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS 0.050U ALPHA-BHC 0.50U METHOXYCHLOR 0.050U BETA-BHC 0.10U ENDRIN KETONE 0.050U DELTA-BHC 0.10U ENDRIN ALDEHYDE 0.050U GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 0.050U HEPTACHLOR 0.050U GAMMA-CHLORDANE /2 o.osou ALDRIN 0.050U ALPHA-CHLORDANE /2 0.050U HEPTACHLOR EPOXIDE 5.0U TOXAPHENE 0.050U ENDOSULFAN I (ALPHA) 1.0UR PCB-1016 (AROCLOR 1016) 0.10U DIELDRIN 2.0U PCB-1221 (AROCLOR 1221) 0.10U 4, 4' -ODE (P, P' -DDE) 1.0U PCB-1232 (AROCLOR 1232) 0.10U ENDRIN 1.0U PCB-1242 (AROCLOR 1242) 0.10U ENDOSULFAN II (BETA) 1.0U PCB-1248 (AROCLOR 1248) 0.10U 4, 4' -DOD (P,P'-DDD) 1.0U PCB-1254 (AROCLOR 1254) 0.10U ENDOSULFAN SULFATE 1.0U PCB-1260 (AROCLOR 1260) 0.10U 4,4'-DDT (P, P' -DDT) \ ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED.FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. *C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE. • liiiiii 'liiiiiil PESTICIDES/PCB'S DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95461 SOURCE, GA PACIFIC CORP HDWD STATION ID, 109-SD ✓ CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 D . NUMBER , KAB 4 BY, D RUMFORD ST, NC 1425 STOP, 00/00/00 08/15/95 * * * *** •• •• •• • • •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS 7.0U ALPHA-BHC 41U METHOXYCHLOR 4.lU BETA-BHC 8.0U ENDRIN KETONE 4.lU DELTA-BHC 8.0U ENDRIN ALDEHYDE 4.lU GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 4.lU HEPTACHLOR 4.lU GAMMA-CHLORDANE /2 4.lU ALDRIN-4.lU ALPHA-CHLORDANE /2 4.lU HEPTACHLOR EPOXIDE 410U TOXAPHENE 4.lU ENDOSULFAN I (ALPHA) BOUR PCB-1016 (AROCLOR 1016) 8.0U DIELDRIN 160U PCB-1221 (AROCLOR 1221) 8.0U 4,4' -DOE (P,P'-DDE) BOU PCB-1232 (AROCLOR 1232) 8.0U ENDRIN BOU PCB-1242 (AROCLOR 1242) 8.0U ENDOSULFAN II (BETA) BOU PCB-1248 (AROCLOR 1248) 8.0U 4,4' -ODD (P, P' -DDD) BOU PCB-1254 (AROCLOR 1254) 8.0U ENDOSULFAN SULFATE BOU PCB-1260 (AROCLOR 1260) 8.0U 4,4' -DDT (P,P'-DDT) 59 PERCENT MOISTURE ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT .ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. *C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE. liiiil PESTICIDES/PCB'S DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS,· GA. *** * •• * •• *. * *. *. * * *. * * * * * *. * •• * *. * * *. * ••• *. * * * * * •• * * *. *. * * * * * •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95462 SOURCE, GA PACIFIC CORP HDWD STATION ID, 013-RN CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, SURFACWA PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 D. NUMBER, KA97 BY, D RUMFORD ST, NC 0700 STOP, 00/00/00 08/15/95 * *. * *** •• •• •• • • •• ***. * * *. *. * * *. *. * * * •• * * * * * * * * * * * * * * *. * * * *. * * * * •• * * * * * * *. * * * * * * *. * *** UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS o.osou ALPHA-BHC .sou METHOXYCHLOR o.osou BETA-BHC O.lOU ENDRIN KETONE o.osou DELTA-BHC O.lOU ENDRIN ALDEHYDE o.osou GAMMA-BHC (LINDANE) CHWRDANE (TECH. MIXTURE) /1 o.osou HEPTACHLOR o.osou GAMMA-CHWRDANE /2 o.osou ALDRIN o.osou ALPHA-CHLORDANE /2 o.osou HEPTACHLOR EPOXIDE 5.0U TOXAPHENE o.osou ENDOSULFAN I (ALPHA) l.OUR PCB-1016 (AROCLOR 1016) O.lOU DIELDRIN 2.0U PCB-1221 (AROCLOR 1221) O.lOU 4,4' -DOE (P, P' -DDE) 1.0U PCB-1232 (AROCLOR 1232) O.lOU ENDRIN 1.0U PCB-1242 (AROCLOR 1242) O.lOU ENDOSULFAN II (BETA) 1.0U PCB-1248. (AROCLOR 1248) O.lOU 4,4' -DOD (P, P' -DDD) 1.0U PCB-1254 (AROCWR 1254) O.lOU ENDOSULFAN SULFATE 1.0U PCB-1260 (AROCLOR 1260) O.lOU 4,4' -DDT (P, P' -DDT) ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. *C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHWRDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHWRDANE. •. Ii I I RECEIVED AUG 2 21995 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region IV Environmental Services Division College Station Road, Athens, Ga. 30613 _u,0 tRFUND SECTION D l***MEMORANDUM****** I . I DATE: 08/05/95 SUBJECT: I I I FROM: I I Results 95-0293 of Metals Analysis; .GA PACIFIC CORP HDWD PLYMOUTH NC CASE NO: 23679 Charles H. Hooper#~/ c,ch; Chief, Laboratory Evaluation/Qualfty I TO: PAT DEROSA Assurance Section ltached are the results of analysis of samples collected as part of ii.he subject project. La result of the Quality Assurance Review, certain data qualifiers ~ay have been placed on the data. Attached is a DATA QUALIFIER 'PORT which explains the reasons that these qualifiers were required. [f you have a.ny questions please contact me. I I I I I ,1 I ATTACHMENT I INORGANIC DATA QUALIFIERS REPORT I Case Number: _.2~3"6,_7,_9~------------- Project Number:~9~5,_-~0"2~9,_3~-----------II Site: GA Pacific Corp Hdwd, Plymouth, NC II Element Flag Samples Affected A. Waters II Be, Cd, II Mn, V Co, Cu, Al, Ba, D Mg, Zn Ca, Fe, D D I R. D H I D I D I a As Pb Hg Cr Pb Pb Se Pb Ni Se J All metals • 11 I I I I I I B. Soils Be, Mn, Al, Mg Cd, Co, V, Zn Ba, Ca, cu, Fe, u u J J J J J u u J J J J u u All positives> IDL, but < CRDL All positives> IDL, but < lOX contaminant level All with Al or Fe concentrations in solution > 150,000 ug/L All with Al or Fe concentrations in solution > 150,000 ug/L All All MDKA93 MDKA81 & 83 MDKA79 MDKA91 MDKA91 MDKA83 All samples All positives> IDL, but < CRDL All positives> IDL, but < lOX contaminant level Reason Baseline instability Positives in blanks Suspected over correction as noted in the contractor res Suspected over correction as noted in the contractor res Matrix spike recovery= 69.5% Blind spike recovery< warning limit % RSC > exposures % RSD > exposures CRDL % RSD > exposures CRDL 20% for 20% for and results 20% for and result Only analysis of 2X required by contract analysis Only analysis of 2X required by contract analysis ICP multiple ICP multiple > IDL, but < ICP multiple > IDL, but < CRDL standard sow for ICP CRDL standard sow for ICP Only analysis of 2X CRDL required by contract SOW analysis standard for ICP Sample pH> 2.0 when received by the laboratory for analysis Baseline instability Positives in blanks I rNORGANIC DATA QUALIFIERS REPORT (continued) I Case Number: _.2._,3,c6._7.!..£<9 _____________ _ ' Project Number:~9~5~-~0~2=9=3 __________ _ I Sit/: GA Pacific Corp Hdwd. Plymouth. NC Element flag Samples Affected I I I I I I I I I I I I I I I I I I Se J All with Al or Fe Sb Zn Ba Ca Cd Cr Co Cu Mg Mn Ni K V K As Sb Ni J J J J R J J R J R J R J R J R J R J J J u u u Concentrations in > 140,000 ug/L All All All All positives All negatives All All positives All negatives All positives All negatives All positives All negatives All positives All negatives All positives All negatives All positives All negatives All All MDKA86 & 87 MDKA82 & 92 MDKA89 MDKA87 solution Reason sllspected over correction in the contractor res as noted Matrix spike recovery= 69% ·serial dilution percent difference= 12.8% Blind spike recovery< warning limit Blind spike recovery< action limit Blind spike recovery< warning limit Blind spike recovery< action limit Blind spike recovery< action limit Blind spike_recovery < action limit Blind spike recovery< action limit Blind spike recovery< action limit Blind spike recovery< action limit Blind spike recovery< warning limit Blind spike recovery< action limit % RSD > 20% for ICP multiple exposures % RSD > exposures CRDL % RSD > exposures CRDL % RSD > exposures CRDL 20% for ICP multiple and results > IDL, but < 23% for ICP multiple and results > IDL, but < 20% for ICP multiple and results > IDL, but < Ii INORGANIC DATA QUALIFIERS REPORT (continued) I Case Nwnber: _,2.,,3,_,6,_7,_9._ ____________ _ Project Nwnber:_;;9~5!..=.!0~2~9~3a..._ __________ _ Site: GA Pacific Corp Hdwd, Plymouth, NC I Jlement Flaa J Samples Affected MDKAB7, as; & 94 I I I I I I I I I I I I I I I As Sb Ni J J MDKA95 MDKA82, 86, 88, 90, 92, 94, & 96 Reason Only analysis of 2X CRDL required by contract SOW analysis Only analysis of 2X CRDL required by contract sow analysis standard for ICP standard for ICP Only analysis of 2X CRDL standard required by contract SOW for ICP analysis METALS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/04/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95444 SOURCE, GA PACIFIC CORP HDWD STATION ID, 017-PB CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, WATER PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 MD NUMBER, KASS BY, D RUMFORD ST, NC 1800 STOP, 00/00/00 ** ** ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L 20UJ 20UJ 4UJ 3UJ lUJ lU 20UJ SUJ 2UJ 4UJ lOUJ 3UJ 40UJ ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM ***REMARKS*** ANALYTICAL RESULTS SAMPLE RECEIVED WITH A PH GREATER THAN 2 ***FOOTNOTES*** UG/L lUJ O.lOUJ SUJ 90UJ 3J 3UJ llOJ S.2U NA 3UJ 2UJ MANGANESE MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM TIN VANADIUM ZINC ***REMARKS*** ANALYTICAL RESULTS *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. --- - - - --- ---- ---- METALS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/04/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95445 SOURCE, GA PACIFIC CORP HDWD STATION ID, 007-SL v CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 MD NUMBER, KA86 BY, D RUMFORD ST, NC 0900 STOP, 00/00/00 ** ** ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** MG/KG 820 6.2UJ 7 42J 0.27U 0.46UJ 2300J 23J 0.78UR 46 28000 26 lOOUJ ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM ***FOOTNOTES*** ANALYTICAL RESULTS MG/KG 66J 0.12U 5.9J 91J 1.1U 1.2U 61 2 .4U NA 5UJ 64J 60 ANALYTICAL RESULTS MANGANESE MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM· TIN VANADIUM ZINC PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS. KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. --- - ---- - - ----- -- METALS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/04/95 *** * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95446 SOURCE: GA PACIFIC CORP HDWD STATION ID: 107-SL CASE NUMBER: 23679 SAS NUMBER: SAMPLE TYPE: SOIL PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/20/95 MD NUMBER: KA87 BY: D RUMFORD ST: NC 0900 STOP: 00/00/00 •• •• ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** MG/KG 880 20UJ 6.2J 48J 0.46U 0.77UJ 2300J 23J 1.3UR 58J 28000 29 120UJ ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM ***FOOTNOTES*** ANALYTICAL RESULTS MG/KG 61J 0.21U 9UJ 130J 1.9U 2.1U no 4U NA 6UJ 83J 76 ANALYTICAL RESULTS MANGANESE MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM TIN VANADIUM ZINC PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER.THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. --------- - ----- -- SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/04/95 METALS DATA REPORT ••• * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *·* * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE SOURCE, GA PACIFIC CORP HDWD STATION ID, 003-SL, CASE NUMBER, 23679 NO. SAS 95447 SAMPLE TYPE, SOIL NUMBER, PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 MD NUMBER, KA88 BY, D RUMFORD ST, NC 0950 STOP, 00/00/00 ** ** ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** MG/KG 4200 3 .4UJ l.8J 41J lU 0.25UJ 1800J 8.9J 2UJ 5UJ . 5900 15 450J ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM ANALYTICAL RESULTS MG/KG 92J 0. 06U 2.2J 270J 0.62U O. 67U 32 1.3U NA 14J 29J 21 ANALYTICAL RESULTS MANGANESE MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM TIN VANADIUM ZINC PERCENT MOISTURE ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE.IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -- - ------ - ---- --- METALS DATA REPORT SAMPLE AND ANALYSIS·MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/04/95 *** * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95448 SOURCE: GA PACIFIC CORP HDWD STATION ID: 005-SL/' CASE NUMBER: 23679 SAS NUMBER: SAMPLE TYPE: SOIL PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/20/95 MD NUMBER: KA89 BY: D RUMFORD ST: NC 1020 STOP: 00/00/00 •• •• •• • • •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** MG/KG 5000 lOUJ 48 190J lU 2UJ 53000J 130J 5UJ 79J 120000 120 llOOJ ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM ***FOOTNOTES*** ANALYTICAL RESULTS MG/KG 380J 0.09U 58J 340J 0.90U 0.97U 130 l.9U NA 20UJ 660J 45 ANALYTICAL RESULTS MANGANESE MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM TIN VANADIUM ZINC PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE.GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. ----ilii iiilil --==-1!!!!1--------------.,__-=· =--=:::::_~•·=•~, METALS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/04/95 ••• •• •• •• •• •• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** PROJECT NO. 95-0293 SAMPLE NO. SOURCE, GA PACIFIC CORP HDWD STATION ID, 006-SL CASE NUMBER, 23679 SAS 95449 SAMPLE TYPE, SOIL NUMBER, PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 MD NUMBER, KA90 BY, D RUMFORD ST, NC 1040 STOP, 00/00/00 •• •• •• • • •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** MG/KG 3900 5.6UJ 11 92J 0.25U lUJ 9300J 28J 3UJ 73J 33000 55 610J ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM ANALYTICAL RESULTS MG/KG 210J 0.58 lOJ 390J lU 1.lU 86 2.lU NA 20UJ 210J 53 ANALYTICAL RESULTS MANGANESE MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM TIN VANADIUM ZINC PERCENT MOISTURE \ ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS.KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -lliii --- --- - --- -- - - - .. METALS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/04/95 *** ** ** ** ** ** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** PROJECT NO. 95-0293 SAMPLE SOURCE: GA PACIFIC CORP HDWD STATION ID: 001-SW / CASE NUMBER: 23679 NO. 95450 SAMPLE TYPE: SAS NUMBER: SURFACEWA · PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/20/95 MD NUMBER: KA91 BY: D RUMFORD ST: NC 1015 STOP: 00/00/00 ** ** ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L ANALYTICAL RESULTS UG/L 440J ALUMINUM 60J 2 OUJ ANTIMONY O . 1 OUJ 4UJ ARSENIC lOJ 28J BARIUM 2200J lUJ BERYLLIUM 3UJ lUJ CADMIUM 3UJ 7200J CALCIUM llOOOJ -5UJ--~~cHROMIUM-------------------------~5uJ 2UJ COBALT NA 6UJ COPPER 4 UJ 910J IRON 2UJ 3J LEAD 2800J MAGNESIUM ANALYTICAL RESULTS MANGANESE MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM------------- TIN VANADIUM ZINC ***REMARKS*** ***REMARKS*** SAMPLE RECEIVED WITH A PH GREATER THAN 2 ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. ---liiiil liiiiil liiii lilliil iliii iiiii liiiiii &iii liiil 111111a METALS DATA REPORT *** * * * * * * * * * * * * *. * •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE SOURCE, GA PACIFIC CORP HDWD STATION ID, 001-SD/" CASE NUMBER, 23679 • • NO. SAS • • • • 95451 NUMBER, • SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. • • • • • • • • • • • • • • • • • • • SAMPLE TYPE, SOIL PROG ELEM, NSF CITY, PLYMOUTH • COLLECTION START, MD NUMBER, KA92 • • • • • • • • • • • COLLECTED BY, D RUMFORD ST, NC 06/20/95 1020 STOP, • • • • • 00/00/00 • • 08/04/95 • • • •• •• •• •• •• • • *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** MG/KG ANALYTICAL RESULTS MG/KG ANALYTICAL RESULTS 17000 ALUMINUM 720J MANGANESE 6.lUJ ANTIMONY O.lOU MERCURY 4U ARSENIC 14J NICKEL lBOJ BARIUM 1900J POTASSIUM 2U BERYLLIUM l.lU SELENIUM lUJ CADMIUM l.2U SILVER 1700J CALCIUM ________ _ ·-30J-----cHROMIUM·--- -----1-30-----SODIUM __ _ 2.3U THALLIUM 20UJ COBALT NA TIN 22J COPPER 5 BJ VANADIUM 31000 IRON 120J ZINC 30 LEAD 57 PERCENT MOISTURE 3200J MAGNESIUM ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. - --- - ---- - --- -- -- METALS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS,' GA. 08/04/95 ***. * * * * *· * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * *** •• •• •• ** •• PROJECT NO. 95-0293 SAMPLE NO. 95452 SOURCE, GA PACIFIC CORP HDWD STATION ID, 101-SW CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, SURFACEWA PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 · MD NUMBER, KA93 BY, D RUMFORD ST, NC 1015 STOP, 00/00/00 •• •• •• •• •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS 550J ALUMINUM 62J MANGANESE 20UJ ANTIMONY 0.10UJ MERCURY 4UJ ARSENIC 5UJ NICKEL 29J BARIUM 2200J POTASSIUM 1UJ BERYLLIUM 3UJ SELENIUM 1UJ CADMIUM 3UJ SILVER 7300J . CALCIUM -SUJ----CHROMIUM·-------------------~-- _________ 110_0_0J __ SODIUM __ 6UJ THALLIUM 2UJ COBALT NA TIN 6UJ COPPER SUJ VANADIUM 990J IRON 2UJ ZINC 3J LEAD 2800J MAGNESIUM ***REMARKS*** ***REMARKS*** SAMPLE RECEIVED WITH A PH GREATER THAN 2 ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN. *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. ----- ------------- METALS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/04/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95453 SOURCE, GA PACIFIC CORP HDWD STATION ID, 101-SD CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 MD NUMBER, KA94 BY, D RUMFORD ST, NC 1020 STOP, 00/00/00 ** ** ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** MG/KG 20000 ALUMINUM 5.7UJ ANTIMONY 4J ARSENIC 190J BARIUM 2U BERYLLIUM lUJ CADMIUM 1700J CALCIUM -25J~---CHROMIUM---- 20UJ COBALT 23J COPPER 32000 IRON 30 LEAD 3200J MAGNESIUM ***FOOTNOTES*** ANALYTICAL RESULTS MG/KG 710J 0.2U 14J 1900J lU MANGANESE MERCURY NICKEL POTASSIUM SELENIUM SILVER l. lU 130_:_ 2.2U NA 59J 120J ~SODIUM---THALLIUM TIN VANADIUM ZINC ANALYTICAL RESULTS 56 PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. illi --- - -- - - -- - -- - - METALS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95454 SOURCE: GA PACIFIC CORP HDWD STATION ID: 004-SL; SAMPLE TYPE: SOIL PROG ELEM: NSF COLLECTED CITY: PLYMOUTH 08/04/95 CASE NUMBER: 23679 SAS NUMBER: COLLECTION START: 06/20/95 MD NUMBER: KA95 BY: D RUMFORD ST: NC 1125 STOP: 00/00/00 MG/KG 3200 ALUMINUM ANTIMONY ANALYTICAL RESULTS *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• •• MG/KG 8.1J 6,9 60J lU lUJ lOOOOOJ -977J~ 2UJ 63J 7800 89 1900J ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM --CHROMIUM _____ -~ --- COBALT COPPER IRON LEAD MAGNESIUM ***FOOTNOTES*** 140J MANGANESE 0.06U MERCURY ANALYTICAL RESULTS 34J NICKEL 500J POTASSIUM 0.60U SELENIUM 0. 64U SILVER 140-----SODIUM--~--- 1. 2U THALLIUM NA TIN 8UJ VANADIUM 510J ZINC 2 3 PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *KoACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -- - - -- - -- - --- - - - - METALS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/04/95 *** ** ** ** ** ** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** PROJECT NO. 95-0293 SAMPLE NO. SOURCE, GA PACIFIC CORP HDWD STATION ID, 002-SL/ CASE NUMBER, 23679 SAS 95455 SAMPLE TYPE, SOIL NUMBER, PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 MD NUMBER, KA96 BY, D RUMFORD ST, NC 1155 STOP, 00/00/00 ** ** ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** MG/KG 4300 ALUMINUM ANALYTICAL RESULTS MG/KG 790J MANGANESE ANALYTICAL RESULTS 4.8UJ ANTIMONY 5.4 ARSENIC 0.09U MERCURY 5.lJ NICKEL 140J BARIUM 370J POTASSIUM lU BERYLLIUM 0.88U SELENIUM lUJ CADMIUM 0.95U SILVER 17000J CALCIUM llJ CHROMIUM---------· ---------3UJ ___ -COBALT 77 __ SODIUM---------------1.~ THALLIUM NA TIN 13J COPPER 20UJ VANADIUM 9200 IRON lOOJ ZINC 250 LEAD 48 PERCENT MOISTURE 660J MAGNESIUM ***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN .VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. --liiiiil ---- -- METALS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/04/95 *** *. * * * * •• *. * *. * * *. * •• * *. * * * * * * * * * * *. * * * * *. * *. * * * * * * * * * * * *. *. * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95456 SOURCE, GA PACIFIC CORP HDWD STATION ID, 009-SW, CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, SURFACEWA PROG ELEM, NSF .COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 MD NUMBER, KA79 BY, D RUMFORD ST, NC 1350 STOP, 00/00/00 •• •• •• •• •• *** * * *. *. * * * *. * * * * * * * * * * * * * * * * * * •• * * * * * * * * * * * * •• *. * * * * * * * * *. * * * * * *** UG/L 1300J 20UJ 4UJ 44J 1UJ 1UJ 8100J 5UJ -2uJ· -- 6UJ 3000J 10J 2900J ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM __ ·coB-ALT COPPER IRON LEAD MAGNESIUM ***REMARKS*** ANALYTICAL RESULTS ------~------- SAMPLE RECEIVED WITH A PH GREATER THAN 2 ***FOOTNOTES*** UG/L 160J 0.2UJ 5UJ 2400J 4UJ 3UJ 11000J ~--6UJ- NA 6UJ 2UJ MANGANESE MERCURY NICKEL POTASSIUM SELENIUM SILVER _SODIUM- THALLIUM TIN VANADIUM ZINC ***REMARKS*** ANALYTICAL RESULTS *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. --liiiil liliiiil -- -- - 111111 --- METALS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/04/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95457 SOURCE, GA PACIFIC CORP HDWD STATION ID, 009-SD - CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 MD NUMBER, KA80 BY, D RUMFORD ST, NC 1425 STOP, 00/00/00 •• •• •• • • •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** MG/KG 12000 ALUMINUM 6.SUJ ANTIMONY 22 ARSENIC 190J BARIUM 2U BERYLLIUM 3UJ CADMIUM 2700J CALCIUM 48J CHROMIUM 20UJ COBALT 100J COPPER 150000 IRON 330 LEAD 2000J MAGNESIUM ***FOOTNOTES*** ANALYTICAL RESULTS MG/KG 970J 0.3U 33J 1200J 1.2UJ 1.3U 120 2.5U NA 48J 530J 58 MANGANESE MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM TIN VANADIUM ZINC ANALYTICAL RESULTS PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. --- -- -- --- ----- METALS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/04/95 ••• • • * • • • • • • • • • • • • • * • • • • • * • • • * • • * * • • * "* * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE SOURCE: GA PACIFIC CORP HDWD STATION ID: 010-SW ✓ CASE NUMBER: 23679 NO. SAS 95458 SAMPLE TYPE: SURFACEWA NUMBER: PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/19/95 MD NUMBER: KA81 BY: D RUMFORD ST: NC 1615 STOP: 00/00/00 •• •• •• • • •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L 480J 20UJ 4UJ 29J lUJ lUJ 7300J 5UJ 2UJ 5UJ 980J 3UJ 2800J ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM ***REMARKS*** ANALYTICAL RESULTS SAMPLE RECEIVED .WITH A PH GREATER THAN 2 ***FOOTNOTES*** UG/L 63J O.lOUJ 5UJ 2300J 3UJ 3UJ llOOOJ 6UJ NA 5UJ 2UJ MANGANESE MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM TIN VANADIUM ZINC ***REMARKS*** ANALYTICAL RESULTS •A-AVERAGE VALUE •NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN •U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. •R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -- --------- ---- -- METALS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/04/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95459 SOURCE, GA PACIFIC CORP HDWD STATION ID, 010-SD, CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 MD NUMBER , KA8 2 . BY, D RUMFORD ST, NC 1620 STOP, 00/00/00 ** ** ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** MG/KG 9900 4.5UJ 3U lOOJ 2U 0. 33UJ 1800J 21J 9UJ 15J 18000 16 1900J ALUMINUM-ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM ***FOOTNOTES*** ANALYTICAL RESULTS MG/KG 450J 0.09U 7.6J 1200J 0.83U 0.89U 80 l.7U NA 33J 64J 42 MANGANESE MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM TIN VANADIUM ZINC ANALYTICAL RESULTS PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO·BE LESS THAN VALUE GIVEN *L-ACTUAL·VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. &ii iiiil -- --- --li!!l!I - METALS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT ·SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/04/95 *** ** ** ** ** ** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** PROJECT NO. 95-0293 SAMPLE NO. SOURCE, GA PACIFIC CORP HDWD STATION ID, 109-SW CASE NUMBER, 23679 SAS 95460 SAMPLE TYPE, SURFACWA NUMBER, PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 MD NUMBER, KA83 BY, D RUMFORD ST, NC 1350 STOP, 00/00/00 ** •• •• •• •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L 660J 20UJ 4UJ 31J 1UJ 1UJ 7400J SUJ 2UJ BUJ 1500J SJ 2700J ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM ***REMARKS*** ANALYTICAL RESULTS SAMPLE RECEIVED WITH A PH GREATER THAN 2 ***FOOTNOTES*** UG/L 87J 0.10UJ SUJ 2200J 3UJ 3UJ 10000J 6UJ NA 6UJ 2UJ MANGANESE MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM TIN VANADIUM ZINC ***REMARKS*** ANALYTICAL RESULTS *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION . &iii ilii ----- ----.. METALS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/04/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ++ ++ ++ ++ ++ PROJECT NO. 95-0293 SAMPLE NO. 95461 SOURCE, GA PACIFIC CORP HDWD STATION ID, 109-SD CASE NUMBER, 23679 SAS NUMBER, SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 MD NUMBER, KA84 BY, D RUMFORD ST, NC 1425 STOP, 00/00/00 ++ ++ ++ ++ ++ *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** MG/KG 11000 6.2UJ 19 160J 2U 2.BJ 2700J 23J 20UJ 130J 70000 250 2000J ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM ***FOOTNOTES*** ANALYTICAL RESULTS MG/KG 650J 0.2U 35J 1200J l.lUJ l.2U 130 2 .4U NA 52J 930J 57 ANALYTICAL RESULTS MANGANESE MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM TIN VANADIUM ZINC PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. fiiii -- ----- -- - --- --,,. '· - METALS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/04/95 *** * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95462 SOURCE: GA PACIFIC CORP HDWD STATION ID: 013-RN CASE NUMBER: 23679 SAS NUMBER: SAMPLE TYPE: SURFACWA PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/19/95 MD NUMBER: KA97 BY: D RUMFORD ST: NC 0700 STOP: 00/00/00 ** ** ** ** ** *** * * * * * * * * t * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L 20UJ 20UJ 3.3U 3UJ 1UJ 2UJ 400UJ 5UJ 2UJ 7UJ 30UJ 3UJ 40UJ ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM ***REMARKS••• ANALYTICAL RESULTS SAMPLE RECEIVED WITH A PH GREATER THAN 2 ***FOOTNOTES*** UG/L 6UJ 0.10UJ 5UJ 90UJ 2.5U 3UJ 210J 5.2U NA 3UJ 130 MANGANESE MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM TIN VANADIUM ZINC ***REMARKS*** ANALYTICAL RESULTS *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. lliil iliii iiii iiiil ---- - - ----- -- I I UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region IV Environmental Services Division College Station Road, Athens, Ga. 30613 l****MEMORANDUM****** I DATE: 08/16/95 SUBJECT: I I FROM: I Results of Purgeable Organic Analysis; 95-0293 GA PACIFIC CORP HDWD PLYMOUTH NC CASE NO: 23679 arlesL~ hief, Laboratory Evaluation/Quality Assurance Section TO: PAT DEROSA 'ttached are the results of analysis of samples collected as part of ife subject project. Isla result of the Quality Assurance Review, certain data qualifiers may have been placed on the data. Attached is a DATA QUALIFIER 'PORT which explains the reasons that these qualifiers were required. 1. If you have any questions please contact me. I ATTACHMENT I I I I I I I I I I I I I I I I I I I I I I I I I ORGANIC DATA QUALIFIER REPORT Case Number 23679 Project Number 95-0293 SAS Number Site ID. Georgia Pacific Corp HDWD, Plymouth, NC Affected Samples Volatiles· all samples 95446 95447,95453, 95455 Extractables 95445,95446 95447,95450, 95452,95454, 95456,95458, 95460,95462 95448 95451 95453,95455, 95459 95455 95457 95461 Compound or Fraction chloromethane benzene toluene chlorobenzene 2-butanone all compounds pyrene benzo(g,h,i)perylene pyrene di-n-octylphthalate benzo(b/k)fluoranthene benzo(a)pyrene indeno(l,2,3-cd)pyrene dibenz(a,h)anthracene benzo(g,h,i)perylene pyrene benzo(b/k)fluoranthene benzo(g,h,i)perylene fluoranthene pyrene benzo(b/k)fluoranthene benzo(g,h,i)perylene benzo(a)pyrene chrysene phenanthrene fluoranthene pyrene chrysene benzo(a)pyrene indeno(l,2,3-cd)pyrene benzo(g,h,i)perylene fluoranthene pyrene chrysene benzo(b/k)fluoranthene benzo(a)pyrene benzo(g,h,i)perylene R J J J J J J J J J J J J J J J J J J J J J J J J J J J J J J J J J J J J Flag Used Reason unacceptable PE sample recovery < quantitation limit < quantitation limit < quantitation limit < quantitation limit exceeded extraction holding time low PE sample recovery low PE sample recovery low PE sample recovery low internal standard recovery low internal standard recovery low internal standard recovery low internal standard recovery low internal standard recovery low internal standard recovery < quantitation limit < quantitation limit low PE sample recovery < quantitation limit < quantitation limit < quantitation limit low PE sample recovery < quantitation limit < quantitation limit < quantitation limit < qunatitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit low PE sample recovery I· I I I I I I I I I I I I I I I I I ORGANIC DATA QUALIFIER REPORT Case Number 23679 Affected Samples Compound or Fraction Pesticides all samples 95445,95446 95447 95454 95455 95457 95459 aroclor-1016 alpha-bhc delta-bhc garnma-bhc 4,4' -DDE 4,4' -DDT beta-bhc 4,4'-DDE delta-bhc garnma-bhc · endrin aldehyde 4,4' -DDE Project Number 95-0293 Flag Used R C C C J J J J J N J J J N Reason unacceptable PE sample recovery GC/MS confirmed GC/MS confirmed GC/MS confirmed < quantitation limit < quantitation limit < quantitation limit < quantitation limit < quantitation limit difference in column quantitations < quantitation limit < quantitation limit < quantitation limit difference in column quantitations PURGEABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95445 SOURCE: GA PACIFIC CORP HDWD STATION ID: 007-SL/ CASE NO.: 23679 SAMPLE TYPE: SOIL SAS NO.: PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/20/95 D. NO.: KA86 BY: D RUMFORD ST: NC 0900 STOP: 00/00/00 ** ** ** ** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG 24UR 240 240 240 1400 sou 240 240 240 240 240 240 240 240 240 240 CHLOROMETHANE BROMOMETHANE ANALYTICAL RESULTS VINYL CHLORIDE CHLO RO ETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE(l,l-DICHLOROETHYLENE) .1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE ***REMARKS*** ***FOOTNOTES*** UG/KG 240 240 240 240 240 240 240 240 240 240 240 240 240 240 240 240 240 59 ANALYTICAL RESULTS 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE). 1,1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES PERCENT MOISTURE ***REMARKS*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. --liill ---- -- --- PURGEABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * *. * * •· * ~ * * * * * * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95446 SOURCE, GA PACIFIC CORP HDWD SAMPLE TYPE, SOIL STATION ID, 107-SL CASE NO., 23679 SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 BY, D RUMFORD ST, NC 0900 STOP, 00/00/00 *** * * * * * *. * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** D. NO., KA87 ** ** ** ** ** UG/KG 27UR 27U 27U 27U 70U 27U 27U 27U 27U 27U 27U 27U 27U 27U 27U 27U ANALYTICAL RESULTS CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLO RO ETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE(l,l-DICHLOROETHYLENE) 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE ***REMARKS*** ***FOOTNOTES*** UG/KG 27U 27U 27U 27U 27U 4J 27U 27U 27U 27U 27U 27U SJ 4J 27U 27U 27U 63 ANALYTICAL RESULTS 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1,1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES PERCENT MOISTURE ***REMARKS*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. 4 R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. --- ---- --- ---- - - - - PURGEABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95· *** * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. SOURCE: GA PACIFIC CORP HDWD STATION ID: 003-SL - 95447 SAMPLE TYPE: SOIL CASE NO.: 23679 SAS NO.: PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/20/95 BY: D RUMFORD ST: NC 0950 STOP: 00/00/00 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG 13UR 13U 13U 13U 20U 40U 13U 13U 13U 13U 13U 13U D. NO.: KASS •• •• • • •• •• 6J 13U 13U 13U CHLOROMETHANE BROMOMETHANE ANALYTICAL RESULTS VINYL CHLORIDE CHLO RO ETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE(l,l-DICHLOROETHYLENE) 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE ***REMARKS*** ***FOOTNOTES*** UG/KG 13U 13U 13U 13U 13U 13U 13U _13U 13U 13U 13U 13U 13U 13U 13U 13U 13U 21 ANALYTICAL RESULTS 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE ' TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1,1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES PERCENT MOISTURE ***REMARKS*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN ,U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. •R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -- ---- ------ -- - PURGEABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95448 SOURCE, GA PACIFIC CORP HDWD STATION ID, 005-SL CASE NO., 23679 SAMPLE TYPE, SOIL SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D. NO., KA89 BY, D RUMFORD ST, NC 1020 STOP, 00/00/00 ** ** ** ** ** *** * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG 17UR 17U 17U 17U 30U 17U 17U 17U 17U 17U 17U 17U 17U 17U 17U 17U CHLO ROM ETHANE BROMOMETHANE ANALYTICAL RESULTS VINYL CHLORIDE CHLO RO ETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE(l,l-DICHLOROETHYLENE) 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE ***REMARKS*** ***FOOTNOTES*** UG/KG 17U 17U 17U 17U 17U 17U 17U 17U 17U 17U 17U 17U 17U 17U 17U 17U 17U 40 ANALYTICAL RESULTS 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1,1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES PERCENT MOISTURE ***REMARKS*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. •R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -;-- ----------- - - .. - PURGEABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95449 SOURCE: GA PACIFIC CORP HDWD SAMPLE TYPE: SOIL STATION ID: 006-SL - CASE NO.: 23679 SAS NO.: PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/20/95 BY: D RUMFORD ST: NC 1040 STOP: 00/00/00 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG ANALYTICAL RESULTS D. NO.: KA90 ** ** ** ** ** NA CHLOROMETHANE NA BROMOMETHANE NA VINYL CHLORIDE NA CHLOROETHANE NA METHYLENE CHLORIDE NA ACETONE NA CARBON DISULFIDE NA 1,1-DICHLOROETHENE(l,l-DICHLOROETHYLENE) NA 1,1-DICHLOROETHANE NA 1,2-DICHLOROETHENE (TOTAL) NA CHLOROFORM NA 1,2-DICHLOROETHANE NA METHYL ETHYL KETONE NA 1,1,1-TRICHLOROETHANE NA CARBON TETRACHLORIDE NA BROMODICHLOROMETHANE ***REMARKS*** NO SAMPLE CONTAINER RECEIVED ***FOOTNOTES*** UG/KG ANALYTICAL RESULTS NA 1,2-DICHLOROPROPANE NA. CIS-1,3-DICHLOROPROPENE NA TRICHLOROETHENE(TRICHLOROETHYLENE) NA DIBROMOCHLOROMETHANE NA 1,1,2-TRICHLOROETHANE NA BENZENE NA TRANS-1,3-DICHLOROPROPENE NA BROMOFORM NA METHYL ISOBUTYL KETONE NA METHYL BUTYL KETONE NA TETRACHLOROETHENE(TETRACHLOROETHYLENE) NA 1,1,2,2-TETRACHLOROETHANE NA TOLUENE NA CHLOROBENZENE NA ETHYL BENZENE NA STYRENE NA TOTAL XYLENES PERCENT MOISTURE ***REMARKS*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. <R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -.. -- --.. -· --- - ---_,_ - PURGEABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** *. * * * •• * *. * * •• * *. *. *. * *. * * * * *. * * * •• * * * * * * *. * * * * * * •• * * * * * * * *. * * *** •• ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95450 SOURCE, GA PACIFIC CORP HDWD SAMPLE TYPE, SURFACEWA STATION ID, 001-SW ••· CASE NO.: 23679 SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 BY, D RUMFORD ST, NC 1015 STOP, 00/00/00 *** * * * * *. *. * •• * *. * *. * * * •• * *. * * * * * * * * * * *. *. * * * * * * *. * * * *. * * * * * * *. * * *** D. NO., KA91 ** •• ** •• ** UG/L 10UR 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U ANALYTICAL RESULTS CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE(1,1-DICHLOROETHYLENE) 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE ***FOOTNOTES*** UG/L 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U ANALYTICAL RESULTS 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1,1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. •R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. --- --·----·---·-- - - PURGEABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95451 SOURCE, GA PACIFIC CORP HDWD SAMPLE TYPE, SOIL STATION ID, 001-SD·- CASE NO., 23679 SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 BY, D RUMFORD ST, NC 1020 STOP, 00/00/00 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** D. NO., KA92 ** ** ** ** ** UG/KG 25UR 25U 25U 25U sou 100U 25U 25U 25U 25U 25U 25U 25U 25U 25U 25U ANALYTICAL RESULTS CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLO RO ETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE(1,1-DICHLOROETHYLENE) 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE ***FOOTNOTES*** UG/KG 25U 25U 25U 25U 25U 25U 25U 25U 25U 25U 25U 25U 25U 25U 25U 25U 25U 60 ANALYTICAL RESULTS 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1,1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE· IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. •R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. ·--- --- -- --- ---- -- -- PURGEABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95452 SOURCE, GA PACIFIC CORP HDWD SAMPLE TYPE, SURFACEWA STATION ID, 101-SW, CASE NO., 23679 SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 BY, D RUMFORD ST, NC 1015 STOP, 00/00/00 *** * * * * * * *. * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** D. NO., KA93 •• •• • • •• •• UG/L 10UR 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U ANALYTICAL RESULTS CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE(1,1-DICHLOROETHYLENE) 1,1-DICHLOROETHANE . 1,2cDICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE ***FOOTNOTES*** UG/L 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U ANALYTICAL RESULTS 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE . 1,1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1,1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES *A-AVERAGE VALUE. *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. - --- -- ---·-- ----- --- PURGEABLE.ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * *. * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO, 95-0293 SAMPLE NO. 95453 SOURCE, GA PACIFIC CORP HDWD STATION ID: 101-SD CASE NO., 23679 SAMPLE TYPE: SOIL SAS NO.: PROG ELEM: NSF COLLECTED CITY, PLYMOUTH COLLECTION START: 06/20/95 D. NO., KA94 BY, D RUMFORD ST: NC 1020 STOP, 00/00/00 ** ** ** ** ** *** *. * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG 22UR 22U 22U 22U JOU JOU 22U 22U 22U 22U 22U 22U 16J 22U 22U 22U ANALYTICAL RESULTS CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLO RO ETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE(1,1-DICHLOROETHYLENE) 1,1-DICHLOROETl!ANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETl!ANE ***FOOTNOTES*** UG/KG 22U 22U 22U 22U 22U 22U 22U 22U 22U 22U 22U 22U 22U 22U 22U 22U 22U 54 ANALYTICAL RESULTS 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1,1,2,2-TETRACHLOROETl!ANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT.ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN •U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. •R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. .. ------------------ PURGEABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95454 SOURCE: GA PACIFIC CORP HDWD SAMPLE TYPE: SOIL STATION -ID: 004-SL , CASE NO.: 23679 SAS NO.: PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/20/95 BY: D RUMFORD ST: NC 1125 STOP: 00/00/00 D. NO.: KA95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• • • •• •• UG/KG 12UR 12U 12U 12U JOU 12U 12U 12U 12U 12U 12U 12U 12U 12U 12U 12U ANALYTICAL RESULTS CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLO RO ETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE(1,1-DICHLOROETHYLENE) 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE ***FOOTNOTES*** UG/KG 12U 12U 12U 12U 12U 12U 12U 12U 12U 12U 12U 12U 12U 12U 12U 12U 12U 20 ANALYTICAL RESULTS 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1,1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. ~R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. --- - ---- --- -- --- -- PURGEABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * *. * * * * * * *. + * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95455 SOURCE, GA PACIFIC CORP HDWD SAMPLE TYPE, SOIL STATION ID, 002-SL · CASE NO., 23679 SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 BY, D RUMFORD ST, NC 1155 STOP, 00/00/00 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** D. NO., KAA96 •• •• •• •• •• UG/KG 17UR 17U 17U 17U 40U 17U 17U 17U 17U 17U 17U 17U 10J 17U 17U 17U ANALYTICAL RESULTS CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLO RO ETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE(1,1-DICHLOROETHYLENE) 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE ***FOOTNOTES*** UG/KG 17U 17U 17U 17U 17U 17U 17U 17U 17U 17U 17U 17U 17U 17U 17U 17U 17U 42 ANALYTICAL RESULTS 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1,1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. ----- ------ - ---- - PURGEABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * *. *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95456 SOURCE, GA PACIFIC CORP HDWD STATION ID, 009-SW - CASE NO., 23679 SAMPLE TYPE, SURFACEWA SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 D. NO., KA79 BY, D RUMFORD ST, NC 1350 STOP, 00/00/00 •• •• • • •• •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L 10UR 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U ANALYTICAL RESULTS CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE(1,1-DICHLOROETHYLENE) 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE ***FOOTNOTES*** UG/L 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U ANALYTICAL RESULTS 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1,1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES •A-AVERAGE VALUE *NA-NOT ANALYZED •NAI-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN •U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. ~R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. ---- - -- - --------!11!1 PURGEABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * *. * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * ••• ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE SOURCE, GA PACIFIC CORP HDWD STATION ID, 009-SD / NO. 95457 SAMPLE TYPE, SOIL CASE NO., 23679 SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 BY, D RUMFORD ST, NC 1425 STOP, 00/00/00 ***. * * * * * * * *. * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** D. NO., KA80 ** ** ** ** ** UG/KG 25UR 25U 25U 25U 40U sou 25U 25U 25U 25U 25U 25U ANALYTICAL RESULTS 27 25U 25U 25U CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE(1,1-DICHLOROETHYLENE) 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE ***FOOTNOTES*** UG/KG 25U 25U 25U 25U 25U 25U 25U 25U 25U 25U 25U 25U 25U 25U 25U 25U 25U 60 ANALYTICAL RESULTS 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1,1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. •R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. --- - ---- -- --- ---1!!11! PURGEABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * ••• * ••• *. * * * * * * * * * * *. * * * *. * * *. *. * ••.•• * * * * •• *. * *. * * * * * * * * * *. * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95458 SOURCE: GA PACIFIC CORP HDWD SAMPLE TYPE: SURFACEWA STATION ID: 010-SW / CASE NO.: 23679 SAS NO.: PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/19/95 BY: D RUMFORD ST: NC 1615 STOP: 00/00/00 D. NO.: KA81 *** *. * •• * *. * *. * * *. * *. *. * *. * * *. * * * •• * * *. *. * * * * * * *. * * * * *. * *. *. * •• *. *** •• •• • • •• •• UG/L lOUR lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU ANALYTICAL RESULTS CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLO RO ETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE(l,l-DICHLOROETHYLENE) 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE ***FOOTNOTES*** UG/L lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU ANALYTICAL RESULTS 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1,1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. ~R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION . --- -- - -- -- -- --.. PURGEABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * * * * *** ** •• ** •• ** PROJECT NO. 95-0293 SAMPLE NO. 95459 SOURCE, GA PACIFIC CORP HDWD SAMPLE TYPE, SOIL STATION ID, 010-SD - CASE NO., 23679 PROG ELEM, NSF COLLECTED CITY, PLYMOUTH · COLLECTION START, 06/19/95 BY, D RUMFORD ST, NC 1620 STOP, 00/00/00 UG/KG 19UR 19U 19U 19U 30U 40U 19U 19U 19U 19U 19U 19U 19U 19U 19U 19U ANALYTICAL RESULTS SAS NO., D. NO., KA82 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLO RO ETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE(l,1-DICHLOROETHYLENE) 1,1-DICHLOROETHANE. 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE ***FOOTNOTES*** UG/KG 19U 19U 19U 19U 19U 19U 19U 19U 19U 19U 19U 19U 19U 19U 19U 19U 19U 47 ANALYTICAL RESULTS 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1,1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES PERCENT MOISTURE *A-AVERAGE VALUE. *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. tR-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.----- - --- -- -- ------- PURGEABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95460 SOURCE, GA PACIFIC CORP HDWD SAMPLE TYPE, SURFACWA STATION ID, 109-SW CASE NO., 23679 SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 BY, D RUMFORD ST, NC 1350 STOP, 00/00/00 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ·* * * * * * * * * * * * * * * * * * * * * *. * * * * *** D. NO., KA83 •• ** •• •• ** UG/L 10UR 10U lOU 10U 10U 10U 10U 10U 10U 10U 10U 10U lOU 10U 10U 10U ANALYTICAL RESULTS CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE(l,1-DICHLOROETHYLENE) 1,1-DICHLOROETHANE . 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE ***FOOTNOTES*** UG/L 10U 10U 10U 10U 10U 10U 10U lOU 10U 10U 10U lOU 10U 10U 10U 10U lOU ANALYTICAL RESULTS 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1,1,2,2-TETRACHLOROETHANE TOLUENE CHLO RO BENZENE ETHYL BENZENE STYRENE TOTAL XYLENE$ *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. •R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. -- --- --- ----- PURGEABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• •• PROJECT NO. 95-0293 SAMPLE NO. 95461 SOURCE, GA PACIFIC CORP HDWD SAMPLE TYPE, SOIL STATION ID, 109-SD CASE NO., 23679 SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 BY, D RUMFORD ST, NC 1425 STOP, 00/00/00 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** D. NO., KA84 •• •• •• • • •• UG/KG 24UR 24U 24U 24U sou 60U 24U 24U 24U 24U 24U 24U 24U 24U 24U 24U CHLOROMETHANE BROMOMETHANE ANALYTICAL RESULTS VINYL CHLORIDE CHLO RO ETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE(1,1-DICHLOROETHYLENE) 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) .CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE ***FOOTNOTES*** UG/KG 24U 24U 24U 24U 24U 24U 24U 24U 24U 24U 24U 24U 24U 24U 24U 24U 24U 59 ANALYTICAL RESULTS 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1,1,2,2-TETRACHLOROETHANE TOLUENE CHLO RO BENZENE ETHYL BENZENE STYRENE TOTAL XYLENES PERCENT MOISTURE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. SR-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION .. ____ _ - -- -- --- --cm --- PURGEABLE ORGANICS DATA REPORT SAMPLE AND·ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** ••• * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** ** ** ** PROJECT NO. 95-0293 SAMPLE NO. 95462 SOURCE, GA PACIFIC CORP HDWD SAMPLE TYPE, SURFACWA STATION ID, 013-RN CASE NO., 23679 SAS NO., PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/19/95 BY, D RUMFORD ST, NC 0700 STOP, 00/00/00 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** D. NO., KA97 ** ** ** ** ** UG/L 10UR 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U ANALYTICAL RESULTS CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLO RO ETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE(1,1-DICHLOROETHYLENE) 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE ***FOOTNOTES*** UG/L 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U ANALYTICAL RESULTS 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1,1,2,2-TETRACHLOROETHANE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. ~R-QC INDICATES THAT DATA·UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR_VERIFICAT~ON•-.----- ----- --- - 11!!!!1 -- --- - PURGEABLE ORGANICS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/15/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• ** ** •• •• PROJECT NO. 95-0293 SAMPLE NO. 95463 SOURCE: GA PACIFIC CORP HDWD STATION ID: 016-TP CASE NO.: 23679 SAMPLE TYPE: SURFACEWA SAS NO.: PROG ELEM: NSF COLLECTED CITY: PLYMOUTH COLLECTION START: 06/19/95 D. NO.: KASS BY: D RUMFORD ST: NC 1300 STOP: 00/00/00 ** •• •• •• •• *** * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L lOUR lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU ANALYTICAL RESULTS CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLO RO ETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE(l,l-DICHLOROETHYLENE) 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE METHYL ETHYL KETONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE ***FOOTNOTES*** UG/L lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU lOU ANALYTICAL RESULTS 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE TRANS-1,3-DICHLOROPROPENE BROMOFORM METHYL ISOBUTYL KETONE METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE) 1,1,2,2-TETRACHLOROETHANE TOLUENE CHLO RO BENZENE ETHYL BENZENE STYRENE TOTAL XYLENES *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES .•J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. ~R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.--------------l!!!l!I ----- I I I I UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region IV Environmental Services Division College Station Road, Athens, Ga. 30613 l****MEMORANDUM****** · I DATE: 08/05/95 SUBJECT: I I FROM: I Results of Spe'cified Analysis; 95-0293 GA PACIFIC CORP HDWD PLYMOUTH NC CASE NO: 23679 Charles H. Hooper ~~~.or~ Chief, Laboratory Evaluation/Quatlty TO: PAT DEROSA Assurance Section 'ttached are the results of analysis of samples collected as part of ihe\subject project. Is a result of the Quality Assurance Review, certain data qualifiers mayihave been placed on the data. Attached is a DATA QUALIFIER IEP\RT which explains the reasons that these qualifiers were required. If you have any questions please contact me. I I I I I I .I ATTACHMENT I I I I I I I I I I I I I I I I I I INORGANIC DATA QUALIFIERS REPORT Case Number:_,2~3=6~7~9,_ _____________ _ Project Number:__.9~5~-~0~2=9:3 __________ _ Site: GA Pacific Corp Hdwd, Plymouth, NC Element A. Waters Be, Cd, Co, Mn, V Al, Ba, Ca, Mg, Zn As Pb Hg Cr Pb Pb Se Pb Ni Se I Ml metals J Soils Be, Cd, Co, ' V, Zn Mn, I Al, ' Mg Ba, Ca, Cu, Fe, Cu, Fe, Flag u u J J J J J u u J J J J u u Samples Affected All positives> IDL, but < CRDL All positives> IDL, but < lOX contaminant level All with Al or Fe concentrations in solution > 150,000 ug/L All with Al or Fe concentrations in solution > 150,000 ug/L All All MDKA93 MDKABl & 83 MDKA79 MDKA91 MDKA91 MDKA83 All samples All positives> IDL, but < CRDL All positives> IDL, but < lOX contaminant level Reason Baseline instability Positives in blanks Suspected over correction as noted in the contractor res Suspected over correction as noted in the contractor res Matrix spike recovery= 69.5% Blind spike recovery< warning limit % RSD > 20% for ICP multiple exposures % RSD > exposures CRDL 20% for ICP multiple and results > IDL, but< % RSD . > exposures CRDL 20% for and result Only analysis of 2X required by contract analysis Only analysis of 2X required by contract analysis Only analysis of 2X required by contract analysis ICP multiple > IDL, but < CRDL standard sow for ICP CRDL standard sow for ICP CRDL standard sow for ICP Sample pH> 2.0 when received by the laboratory for analysis Baseline instability Positives in blanks ·I I I I I I I I I I I I I I I I I I I INORGANIC DATA QUALIFIE~ REPORT (continued) Case Nwnber:~2=3~6~7~9~------------- Project Number:~9~5~-~0~2~9~3~----------- Site: GA Pacific Corp Bdwd, Plymouth, NC Element Se Sb Zn Ba Ca Cd Cr Co Cu Mg Mn Ni K V K As Sb Ni Flag J J J J J R J J R J R J R J R J R J R J J J u u u Samples Affected All with Al or Fe Concentrations in solution > 140,000 ug/L All All All All positives All negatives All All positives All negatives All positives All negatives All positives All negatives All positives All negatives All positives All negatives All positives All negatives All All MDKA86 & 87 MDKA82 & 92 MDKA89 MDKA87 Reason Suspected over correction as noted in the contractor ICS Matrix spike recovery = 69% Serial dilution percent difference 12.8% Blind spike recovery < warning limit Blind spike recovery < action limit Blind spike recovery< warning limit Blind spike recovery< action limit Blind spike recovery< action limit Blind spike recovery < a.ction limit Blind spike recovery< action limit Blind spike recovery< action limit Blind spike recovery< action limit Blind spike recovery< warning limit Blind spike recovery< action limit % RSD > 20% for ICP multiple exposures % RSD > 20% for ICP multiple exposures and results > IDL, but < CRDL % RSD > 23% .for ICP multiple exposures and results > IDL, but < CRDL % RSD > 20% for ICP multiple exposures and results > IDL, but < CRDL ·I I I I I I I I I I I I I I I I I I I INORGANIC DATA QUALIFIERS REPORT (continued) Case Number:_;;2~3~6~7Ll9'--------------- Project Number:_a9~5~-~0~2~9=--=.3 __________ _ Site: GA Pacific Corp Hdwd, Plymouth, NC Element As Sb Ni Flag J J J Samples Affected MDKA87, 88, & 94 MDKA95 MDKA82, 86, 88, 90, 92, 9.4, & 96 Reason Only analysis of 2X required by contract analysis CRDL standard SOW · for ICP Only analysis of 2X CRDL required by contract sow analysis standard for ICP Only analysis required by analysis of 2X CRDL standard contract sow for ICP SPECIFIED ANALYSIS DATA REPORT SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/04/95 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ** •• ** •• PROJECT NO. 95-0293 SAMPLE NO. 95469 SAMPLE TYPE: SEDIMSPK SOURCE: GA PACIFIC CORP HDWD PROG ELEM: NSF COLLECTED BY: ESAT STATION ID: 0022790 CASE.NO.: 23679 SAS NO.: CITY: PLYMOUTH ST: NC COLLECTION START: 00/00/00 STOP: 00/00/00 D. NO.: MD NO: KA78 •• ** ** ** •• *** * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ***FOOTNOTES*** RESULTS UNITS PARAMETER 150 MG/KG CYANIDE *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. ~ --- -----11!!!1!!1 -----