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HomeMy WebLinkAboutNCD000813592_19920201_GA-Pacific Corp Hdwd Saw_SERB PA SI_Phase II Screening Site Inspection Volume I-OCRI le I I I I I I I II I I I I I I I -,._ I Sl'ATE Of' NORTH CljtROLINA - Depa,·t,nent of Environment, 1-Iealth, and Natural Resources Division of Solid Waste ltlra11agen1ent Superfund Section Georgua Pacific Corporation Hardwood Sawmill NCD 000813592 Phase II Screening Site Inspection Volun1e I Septemberl 991 By: Greenhorne & O'l\tara, Inc. I It I I I I I I I :f I I I I I I I PHASE II SCREENING SITE INVESTIGATION FOR THE GEORGIA PACIFIC CORPORATION HARDWOOD SAWMILL PLYMOUTH, NORTH CAROLINA NCD 000813592 Submitted to: State of North Carolina Department of Environment, Health, and Natural Resources Division of Solid Waste Management Superfund Section Raleigh, North Carolina Prepared By: Greenhorne & O'Mara, Inc. 9001 Edmonston Road Greenbelt, Maryland 20770 September 1991 Revised February 1992 CERCLA I ' I I I I I I I ' I I I I I I ~ I I TABLE Of CONTENTS EXECUTIVE SUMMARY ••••••••••••••••••••••••••••••••••••••••••••••••••••• 1 1. 0 INTRODUCTION ••••••••••••••••••••• '. •••••••••••••••••••••••••••••••• 2 1. 1 OBJECTIVES •••••••••••••••••••••••••••••••••••••••••••••••••••• 2 1. 2 SCOPE OF WORK ••••••••••••••••••••••••••••••••••••••••••••••••• 2 2. 0 SITE CHARACTERIZATION ••••.••••••••••••••••••••••••••••••••••••••••• 4 2 .1 SITE BACKGROUND AND HISTORY ••••••••••••••••••••••••••••••••••• 4 2. 2 SITE DESCRIPTION ••••••••••••••••••••••••••••.••••••••••••••••• 4 2.2.1 Site Location ........•.•.••..••..•........•...•...••••. 4 2.2.2 Site Features .•.....•...•..•......•.......••..•••.•.••• 4 2.2.3 Waste Characteristics ••••••••••.•.•......•••...•..••••• 5 3 • 0 ENVIRONMENTAL SETTING •••••••••••••••••••••••••••••.••••••••••••••• 7 3 .1 TOPOGRAPHY •••••••••••••••••••••••••••••••••••••••••••••••••••• 7 3. 2 SURFACE WATER ••••••••••••••••••••••••••••••••••••••••••••••••• 7 3.2.1 Overland Drainage and Affected Water Bodies .........•... 7 3.2.2 Climatology ......•..............•...•..........•....•... 7 3 .3 GROUNDWATER ••••••••••••••••••••••••••••••••••••••••••••••••••• 7 3. 3 .1 Hydrogeology ...•.•..••...•.• , ......•.......•....•.•..•.. 7 3.3.2 Aquifer Use .......•..•...•..•......•.......•...••....•.. 8 3. 3 . 3 Soils ......•.....•...•...•..•..............•.........••. 8 3. 4 POPULATION DISTRIBUTION ••••••••••••••••••••••••••••••••••••••• 9 3.5 WATER SUPPLY •••••••••••••••••••••••••••••••••••••••••••••••••• 9 3.6 LAND USE ••••••••••••••••••••••••••••••••••••••••••••••••••••• 10 3. 7 SENSITIVE ENVIRONMENTS ••••••••••••••••••••••••••••••••••••••• 10 4. 0 FIELD INVESTIGATION •••••••••••••••••••••••••••••••••••••••••••••• 11 4.1 DESCRIPTION OF SAMPLES AND SAMPLE LOCATIONS •••••••••••••••••• 11 4. 2 FIELD MEASUREMENTS ••••••••••••••••••••••••••••••••••••••••••• 11 4. 3 ANALYTICAL RE SUL TS ••••••••••••••••••••••••••••••••••••••••••• 11 5. 0 CONCLUSIONS AND RECOMMENDATIONS •••••••••••••••••••••••••••••••••• 14 REFERENCES APPENDIX A APPENDIX B APPENDIX C MAPS, PHOTOGRAPHS AND TABLES SITE INSPECTION FORM ANALYTICAL DATA I I I I I I I ' I I I I I I I EXECUTIVE SUMMARY The Georgia Pacific Corporation Hardwood Sawmill site is a 25-acre site located off of Plywood Drive within Plymouth city limits, in \lashing ton County. It was previously owned by Atlas Plywood and operated as a plywood plant. In 1950, the Georgia-Pacific Corporation purchased the site, demolished the existing structures, and developed a planer-sawmill-office facility. The facility was primarily engaged in sawing and planing rough hardwood lumber and timber from logs. After a fire in 1983, the plant permanently closed and operations ceased. The site was later used by Outer Banks Contractors for an asphalt operation. It is currently unoccupied and inactive. Process wastes associated with operations at the Georgia Pacific facility consisted primarily of spent oil, spent halogenated degreasing agents, spent nonhalogenated solvents, bottom sediment sludge from wood preserving processes, and an insecticide formulation. The wood preservative used contained pentachloropheneate, sodium metaborate, and other chlorophenols; the insecticide formulation contained lindane. During_ the wood treatment process, lumber was passed through a dip vat on a conveyor system and allowed to drip dry onto the ground. The Georgia Pacific Hardwood Sawmill is located withil) the Atlantic Coastal Plain Physiographic Province. It is located adjacent to the Roanoke River in a region characterized by extensive, flat coastal swamps and marshes. The primary geologic units identified in the Plymouth area are Tertiary rocks of the Coastal Plain referred to as the Yorktown Formation and the Duplin Formation. The Yorktown Formation is a confined aquifer which serves as the chief source of water supply for the eastern part of \lashington County. On December 6, 1985, NCDHR/DHS completed a Preliminary Assessment on the Georgia Pacific plant and recommended that the site be inspected on a low priority basis. NUS Corporation conducted an off-site reconnaissance and a Phase I Screening Site Inspection (SSI) on _October 11, 1989, and' recommended that no further action be planned for the site. On July 11, 1991, Greenhome & O'Hara Inc., under contract with NCDEHNR, conducted a Phase II SSI. A total of nine (9) environmental samples were taken at the site. Results of the sampling event indicate that releases of contaminants have occurred around the facility. Due to the presence of wetlands, fisheries, and recreational activities downstream in the Roanoke River and Albemarle Sound, G&O is recommending that the site move onto the next stage of the pre-remedial process. 1 I ' I I I I I I I , I I I I I I I 1.0 INTRODUCTION 1. 1 OBJECTIVES Greenhorne and O'Hara, Inc. (G&O) conducted a Phase II Screening Site Inspection (SSI) at the Georgia Pacific Corporation Hardwood Sawmill site located in Plymouth, Washington County, North Carolina. The overall objective of the Phase II SSI is to provide information to determine whether a site should move onto the next stage of the pre-remedial process or be designated as "no further remedial action planned (NFRAP)" under the Federal Superfund program. Additional objectives of the Phase II SSI are the following: 0 0 0 0 Identify the types of contaminants present. Assess whether a release of hazardous substances has occurred; Search for evidence of actual human and environmental exposure to contaminants. Determine the likelihood of the site scoring high enough on the HRS to be recommended for further pre-remedial action under the Federal Superfund program. The SSI builds upon data obtained during the preliminary assessment (PA) and Phase ISSI stages to further characterize problems at or near the site and to support a management recommendation. 1.2 SCOPE OF VORK The scope of work for the Phase II 551 includes the following tasks: 0 0 0 0 Reviewing both EPA and state file material. Preparing an abbreviated site-specific sampling plan and Health and Safety Plan. This task included developing · a site map to illustrate proposed sampling locations, the approximate number of samples, and the type of samples to be collected. Conducting a site reconnaissance with the NCDEHNR to determine and flag actual sampling locations based on the sampling plan and existing field conditions, and the professional judgement of the NCDEHNR and the G&O sampling team. During the site reconnaissance, G&O also developed a site layout map to illustrate all of the important site features including location of buildings, access roads, and waste source areas, as well as site drainage. Performing field sampling activities by collecting up to five (5) environmental media samples and three (3) QA/QC samples. The five environmental samples usually included two (2) groundwater samples (with a maximum well depth of 15 feet) and three (3) surface soil samples. The three (3) QA/QC samples included one (1) water duplicate, one (1) surface soil duplicate, and one (1) trip blank. 2 I ' I I I I I I I ' I I I I I I I 0 0 Analyzing laboratory data and presenting the data in four summary tables: volatile organic compounds, semi-volatile organic compounds, inorganic compounds, and pesticides/PCBs. Any releases that were observed were highlighted on the tables and discussed in the Phase II SSI report. Preparing a Phase II SSI report that presents information gathered during the site visit, field observations, and laboratory data with respect to observed releases. Any existing data gaps will be discussed in the text. Greenhorne and O'Mara was not contracted to collect additional background information. 3 I I I I I I I ' I I I I I I It I I 2.0 SITE CHARACTERIZATION 2.1 SITE BACKGROUND AND HISTORY The Georgia Pacific Corporation Hardwood Sawmill site is a 25-acre parcel of land previously owned by Atlas Plywood. In 1950, the Georgia Pacific Corporation purchased the site, demolished the existing structures, and developed a planer-sawmill-office facility (Ref. 2) The facility was primarily engaged in sawing and planing rough hardwood lumber and timber from logs (Ref. 3). After a fire in 1983, the plant pe'rmanently closed and operations ceased (Ref. 2). In 1989, the site was owned by Decatur Part_nerships of Naggshead, North Carolina and was leased to Outer Banks Contractors, Inc. Plant Number 4, an asphalt operation (Ref. 4). The site is currently owned by Outer Banks Contractors (Ref. 9). The Georgia Pacific facility submitted a RCRA Part A application for a hazardous waste permit on November 12, 1980 (Ref. 3). In August of 1982, the facility's status was changed from a treatment/storage/disposal (TSO) and generator facility to a small-quantity generator. According to NCDHR representatives, the Georgia Pacific facility is currently listed as a conditionally exempt, small-quantity generator (less than 250 pounds per month) due to its inactive status. No remedial activities have been performed at this facility (Ref. 1, 6). On December 6, 1985, the North Carolina Department of Human Resources/Division of Health Services (NCDHR/DHS) completed a preliminary assessment report on the Georgia Pacific Hardwood Sawmill plant. The report concluded that because it had been in operation for at least 35 years and since past waste handling practices were unclear, the site should be inspected on a low priority basis (Ref. 2). NUS Corporation conducted an off-site reconnaissance on October 11, 1989, and subu1itted a Phase I Screening Site Inspection (SSI) to EPA on August 20, 1990 (Ref. 1, 7). Based on the low probability that drinking water would be impacted by prior waste handling practices, the NUS report recommended that no further remedial action be planned for the site (Ref. 1) . 2.2 SITE DESCRIPTION 2.2.1 Site Location The Georgia Pacific site is located off of Plywood Drive within Plymouth city limits, in Washington County (Appendix A, Figure 1). The site can be found on the Plymouth East and Westover, N.C. USGS 7.5' Quadrangle Maps at latitude 35° 52' 30'N and longitude 76° 44' 30"W (Ref. 8) • 2.2.2 Site Features The property consists of approximately 25 acres. NUS Corporation conducted an off-site reconnaissance on October 11, 1989 and noted that the facility was accessible by way of wooded areas surrounding the site. They 4 I ' I I I I I I I ' I I I I I I ' I I noted that the main entrance was off of Plywood Drive and was blocked by a metal gate during non-operational hours. NUS prepared a site sketch, which included an office building, other unidentified buildings, air emissions stacks, two storage tanks, a sand mound, a weigh house, tanks, and Georgia Pacific planer and sawmill buildings (Ref. 7). On July 11, 1991, Greenhorne & O'Mara staff conducted an on-site reconnaissance and carried out a sampling plan on the Plymouth site. The site was presently unoccupied, but many of the buildings and structures used by the former occupants were still present, including the sawmill, the boiler house, the machine shop, and smoke stacks (Photograph 8). Few remains of the green chain system were visible. The green chain system was deScribed by a site representative to be the conveyor system that carried the cut lumber from the sawmill, through a dip tank process, and finally into the holding area. Wood from the former green chain structure (Photograph 5) and the some of the old belts from the conveyor system (Photograph 6) were identified on the site, as well as the concrete pads which were used as temporary stacking areas (Photograph 2, 7). No signs of contamination were noted in this area (Ref. 9). A site representative also indicated that the former plywood plant, employing approximately 400 workers, was located adjacent to the sawmill. He also indicated that approximately 10 employees worked on the site during the time of the asphalt operation. An alleged spill of TCE occurred during the time of the asphalt operation; the vegetation in this area appeared to be stressed and blotchy (Ref. 9). 2.2.3 Waste Characteristics Operations at the Georgia Pacific facility included the production of treated and nontreated hardwood lumber (Ref. 3, 10). Process wastes associated with the plant consisted primarily of spent oil (DOOO- ignitable/D007-chromium, D008-lead), spent halogenated degreasing agents (FOOl), spent nonhalogenated solvents (F003, FOOS), bottom sediment sludge from the treatment of wastewaters from the wood preserving processes, and an insecticide formulation (Ref. 1). The preservative used, Noxtane (trade name); was manufactured by the Koppers Company of St. Louis and contained pentachloropheneate, sodium metaborate, and other chlorophenols. The insecticide formulation contained lindane (Refs. 1, 3, 10, 11, 12). During the process of wood preserving, lumber was passed through a dip vat on a conveyor system. After removal from the preservative or insecticide formulation, the wet wood was allowed to drip dry onto the ground, thus contaminating the soil (Ref. 1, 10). Annual waste production at the facility included 20,000 pounds of DOOO, D007, and D008 waste, 16,300 pounds of KOOl waste (bottom sediment sludge from the treatment of wastewaters from wood preserving processes that use pentachlorophenol) with lindane, and 375 pounds of FOOl, F003, FOOS waste (Ref. 1, 3). A RCRA Part A application indicated that the wastes were stored in drums (Ref. 1, 3). During a RCRA Inspection· conducted on October 1981, representatives from the North Carolina Department of Human Resources (NCDHR) discovered that the wastes were being burned in the facility boilers and/or sent to the county landfill (Ref. 1, 10). It was also noted during the inspection that the wood treatment process involved spilling waste directly on the ground (Ref. 1, 10). A tank used in the wood 5 I I I I I I I ' I I I I I I ' I I treatment process was also found to be leaking (Ref. 10, 13). Remedial action plans were initiated by NCDHR in November 1981, but no remedial activities have been performed at the facility (Ref. 6, 14). 6 I ' I I I I I I I ' I I I I I I I 3.0 ENVIRONMENTAL SETTING 3.1 TOPOGRAPHY The Georgia Pacific Hardwood Sawmill site is on a relatively flat parcel of land surrounded by the Roanoke River on the northwest and wetlands around the remainder of the property. It is located in a region characterized by extensive, flat coastal swamps and marshes. According to USGS Quadrangle maps, elevations in the vicinity of the site are slightly above 5 feet National Geodetic Vertical Datum (NGVD) around the facility and slightly below 5 feet NGVD in the nearby wetland areas (Figure 3 and Ref. 8). 3.2 SURFACE WATER 3.2.1 Overland Drainage and Potentially Affected Water Bodies The green chain conveyor system and dip tank were formerly located approximately 250 feet south of the banks of the Roanoke River. Generally, runoff from the site drains to adjacent wetlands and ditches as well as to the Roanoke River. The Roanoke River flows northeast for approximately 5.7 miles and empties into Albemarle Sound, which flows east for the remainder of the 15-mile migratory pathway (Ref. 8). The Roanoke River is classified as a nclass en river with an "Sw" or Swamp Water supplemental classification (Ref. 35). Class C waters are protected for aquatic life propagation and survival, fishing, wildlife, secondary recreation, and agriculture. Swamp waters have low velocities and other characteristics which are different from adjacent streams. Albemarle Sound, in the vicinity of Bachelor Bay ( see Figure 1), is classified as a 'Class B Sw' water body, denoting primary recreation and any other usages specified by the C classification (Ref. 35). Common fish caught in the area are the spot clocker, the catfish, the American and hickory shed, the white perch, the strip bass, and the blue back (Ref. 15). There are no surface water intakes for municipal drinking water supplies within 15 miles downstream of the site (Ref. 1, 8). ' 3.2.2 Climatology Northwestern Washington County has approximately 50 inches and a mean annual 41 inches (Ref. 16). Therefore, the net The 2-year, 24-hour rainfall in this area 17) . 3.3 GROUNDWATER 3.3.1 Hydrogeology a mean annual precipitation of lake evaporation of approximately annual precipitation is 9 inches. is approximately 4.0 inches (Ref. The site is located within the Atlantic Coastal Plain Physiographic Province, which is characterized by complexly interbedded sediments. The sediments are unconsolidated and consist primarily of sand, silt, and clay transported by streams from the adjoining uplands of the Piedmont and Blue 7 I I I I I I I ' I I I I I I I Ridge Provinces. The geologic formations dip towards the coast (Ref. 18). The primary geologic units identified in the Plymouth area are Tertiary rocks of the Coastal plain referred to as Yorktown Formation and the Duplin Formation (Ref. 19). The Yorktown Formation in North Carolina includes three members: the Sunken Meadow Member, the Rushmere Member, and the Morgarts Beach Member. The Sunken Meadow Member consists of a fine, moderately to well-sorted sand containing 5 to 15 percent silt and 1 percent clay. Large mollusks are common in this member. The Rushmere Member overlies the Sunken Meadow Member and is typically moderately well sorted fine-grained sand. Phosphate and glauconite are common in the Rushmere Member in amounts less than 10 percent. Shell-rich beds are also common. The uppermost part of the three Yorktown members is the Morgarts Beach Member which is described as very fine-grained, with silt and clay content up to 60 percent. The Duplin Formation is a sandy, calcareous, fossiliferous unit. It includes fossiliferous sand, sandy limestone, silty limestone, and calcareous silty sand (Ref. 19). 3.3.2 Aquifer Use East of Plymouth, in the Town of Roper, a typical cross section of the underlying strata includes 15 feet of surficial deposits, 200 feet of sand and marl of the Yorktown Formation, and then the limestones of the Castle Hayne Formation. The surficial deposits aquifer is usually unconfined and is rarely used for potable water supplies. The Yorktown Formation is a confined aquifer, which serves as the chief source of water supply for the eastern part of Washington County. Although the section thins from east to west, the Yorktown Formation is present under Plymouth (Ref. 19). The Castle Hayne aquifer is generally a confined formation and it is the most productive aquifer in North Carolina (Ref. 20). It is the principal source of water supply in the western part of the county. The aquifer consists of porous and permeable limestone and lies at a depth ranging from about 120 feet in the western part of the county to 400 feet in the eastern part of the county (Ref. 19). The Castle Hayne aquifer is used in the Plymouth area and it can be reached between 150 feet to 180 feet below land surface (bls). Due to large withdrawals in recent years, the artesian effects have been eliminated (Ref. 23). Depth to groundwater is generally 28 feet bls. However, the site is located adjacent to the Roanoke River and the water level measured during the July, 1991 sampling event was between 3.5 and 5 feet bls (Ref. 9). The layer of marl and sand found in Plymouth represents the layer of lowest hydraulic conductivity between the aquifer and the surface. Marl and sand of this type have been shown to have 1 x 10-5 to 1 x 10-7 cm/sec (Ref. 24). 3.3.3 Soils The soils on the Georgia Pacific site are primarily Tarboro sands with a slope of Oto 3 percent. The soils in the wetlands adjacent to the site are Muckalee loams (Ref. 25). Tarboro sand is an excessively drained soil normally found on low broad ridges commonly adjacent to Albemarle Sound and the Roanoke River. The surface layer of this soil is low in organic matter content. Permeability is rapid, and the available water capacity is low. a I I I I I I I ' I I I I I I ' I I The soil is well suited to most urban uses and provides a good support for most structures. Muckalee loams, found in the small stream surrounding the property, is a nearly level, poorly-drained hydric soil found on floodplains and small streams in this region. It is subject to frequent flooding (Ref. 25). 3.4 POPULATION DISTRIBUTION The City of Plymouth currently has a population density of 1,138.9 persons per square mile (Ref. 27). To determine the population within unincorporated areas of Washington County, a house count was conducted from the USGS quadrangle maps. The number of houses was then multiplied by 2. 72, which is the 1990 average number of residents per household in Washington County (Ref. 27). The number of residents within each radius ring was then calculated and the values were added to provide a cumulative population. Since the site is currently unoccupied and inactive, there was no on-site population. The table below summarizes the calculated total population (Ref. 28): Radius Population/Radii Cumulative Population 1/4-mile 421 421 1/2-mile 524 945 1-mile 1,295 2,240 2-mile 2,242 4,482 3-mile 2,091 6,573 4-mile 1,599 8,172 3.5 WATER SUPPLY Groundwater is the only source of potable water in Washington County. Only the Towns of Roper and Plymouth have public water supplies (Ref. 25). Residents within a 4-mile radius of the site obtain their water supply from one of three sources: the City of Plymouth Public Works Water System, the Washington County system (which obtains water from the City of Plymouth), and private well use (Ref. 1, 7). The City of Plymouth Public Works Water System uses four wells having an average depth of approximately 175 feet; three of the wells are located inside the city limits and the fourth is located within one mile of the city limits. All the wells are located between 1 to 2 miles south of the site and the total population served is approximately 5,000 residents (Ref. 1, 8, 29). The water system also has two tanks: a 250,000 gallon capacity tank at the Fork of Hobkins, Roosevelt, and a 500,000 gallon tank on Eastman Street (Ref. 7). The Washington County system connects to the Plymouth system and serves unincorporated areas as shown in Figure 3 (Ref. 7, 30). The county system serves 3,900 residents· (Ref. 29). The remainder of the residents living within a 4-mile radius of the site rely on private wells for their water supply. Private wells within the study area are generally 200 feet deep. The closest private well is located on Route 1 approximately 2.7 miles from the facility (Ref. 1, 7). The total population using groundwater is 9 I I I I I I I ' I I I I I I ' I I estimated below (Ref. 28): Population relying on groundwater for potable water Radius Population/Radii Cumulative Population On-site 0 0 1/4-mile 0 0 1/2-mile 0 0 1-mile 0 0 2-mile 8,919 8,919 3-mile 316 9,235 4-mile 628 9,863 3.6 LAND USE Access to the site is limited by fencing and a gate ·guardhouse (Ref. 1, 7). The nearest residence is located approximately 700 feet east of the facility. Plymouth High School is located on the property approximately 700 feet south of the facility, Also, a baseball park and a residential area are adjacent to the facility (Ref. 1, 7). Land northeast of Plymouth and north of the Roanoke River is primarily uninhabited wetlands (Ref. 1, 8) • 3.7 SENSITIVE ENVIRONMENTS There are no known critical habitats of Federally-listed endangered species in the vicinity of the site (Ref. 31). There are, however, several endangered and threatened species identified in the county. The bald eagle is a federally and state-designated endangered species; and the Waccamaw killifish and golden eagle are state-designated endangered and threatened species, respectively (Ref. 1, 32). There are also extensive wetland areas in the vicinity.of the site. Approximately half of the 4-mile radius study area is covered by wooded marsh or swamp (Ref. 8). The river and sound may also be spawning areas, migratory pathways or feeding areas for fish species. 10 I I I I I I I ' I I I I I I I 4.0 FIELD INVESTIGATION 4.1 DESCRIPTION OF SAMPLES AND SAMPLE LOCATIONS A total of nine (9) environmental samples were collected to characterize the site. To determine whether a release of contaminants has occurred, limited subsurface and surficial investigation was recommended to obtain soil, groundwater, and sediment samples for laboratory analysis. The locations of the sampling points were originally proposed in an abbreviated sampling plan prepared by G&O; however, the NCDEHNR made the final recommendations during the sampling event conducted on July 11, 1991. Therefore, the final sampling locations as shown in Appendix A, Figure 2 reflect the decision of the NCDEHNR staff. To determine whether contaminants were released into the environment, two ( 2) surface soil samples ( SSOl and SS02) and three ( 3) groundwater samples (G\,101, G\,102, and G\,103) were obtained by G&O personnel. Surface soil sample SS02 was a composite of three locations. A representative of the NCDEHNR collected two (2) surface soil samples and two (2) sedi.ment samples from the locations shown on the site layout and sampling map (Appendix A, Figure 2 and Photographs 1 through 10). All the samples collected on the site were contained, preserved, and held in accordance with the Standard Operating Procedures (SOP) (Ref. 33). 4.2 FIELD MEASUREMENTS Field measurements collected for groundwater samples include temperature and conductivity. These values are listed in Table 1. SAMPLE CODE GWGWOl GWGW03 TABLE 1 FIELD MEASUREMENTS FOR GROUNDWATER SAMPLES GEORGIA PACIFIC HARDVOOD SAVKILL PLYMOUTH, VASHINGTON COUNTY, NORTH CAROLINA p.11 5.5 7.0 TEMPERATURE Cllcl 26.6-29.0 23.7-24.9 CONDUCTIVITY lnmhos/cml 0.80-0.81 2.03-2.24 4.3 ANALYTICAL RESULTS Upon completion of the sampling event, the G&O samples were taken for analysis to Industrial and Environmental Analysts, Inc. ( IEA) in Research Triangle Park, North Carolina (see Volume II). Level IV Routine Analytical Service (RAS) Contract Laboratory Program (CLP) data packages and associated narratives were assembled for this project by IEA. The IEA analytical data was validated by NUS Corporation. The NCDEHNR samples were 11 I I ' I I I I I I '-I I I I I I I 18 I were taken to the State Laboratory of Public Health in Raleigh for analysis. The results of the sample analysis are summarized in Tables 2A and 2B (Appendix B) and discussed below. I. DOWNGRADIENT GROUNDWATER (GWGW02) A groundwater sample was collected from a hand-augured temporary.well located in the green chain area. No Volatile organic Compounds (VOCs) or Semi-Volatile Organic Compounds (BNAs) were detected above CRDL in this sample. Alpha BHC (0.12 ppb), beta BHC (0.045J ppb), delta BHC (0.13 ppb) and gamma BHC (lindane) (0.32 ppb) were the only PCBs and/or Pesticides reported significantly higher than background in this sample. Several inorganics were identified and reported in the groundwater sample; however only beryllium and manganese were detected in significant concentrations (greater than 3x above the background concentration). The beryllium exceeded the Federal Maximum Contaminant Level (MCL) of 1 ppb and manganese exceeded the NCMCL (50 ppb). DOWNGRADIENT GROUNDWATER (GWGW03) A groundwater sample was collected from a hand-augured temporary well located in the TCE area. Chloroethane ( 990 ppb) was the only Volatile Organic Compound (VOC) reported significantly higher than background in this sample. No Semi-Volatile Organic Compounds (BNAs) were detected above CRDL in this sample. No PCBs and/or Pesticides were reported in this sample. Several inorganics were identified and reported in the groundwater sample; however only arsenic, manganese and sodium were detected in significant concentrations (greater than 3x above the background concentration). GREEN CHAIN AREA COMPOSITE (GWSS02) -A composite soil sample was collected in the green chain area at the site. No voes or BNAs were reported in this sample. Alpha BHC (470 ppb), delta BHC (480 ppb), gamma BHC (lindane) (980 ppb) and 4,4'-DDD (170C ppb) were the only PCBs and/or Pesticides reported significantly above background in this sample. Barium (320 ppm), calcium (79000 ppm), cobalt (5.3 ppm), copper (23 ppm), lead (33 ppm), magnesium (3600 ppm), manganese (850 ppm) and potassium (1800 ppm) were the only inorganics reported in significant concentrations in this sample. Note: The following four samples were collected by NCDEHNR personnel and analyzed by the State Laboratory of Public Health. TRANSFORMER STATION AREA COMPOSITE (GWSS03) A composite soil sample was collected in the transformer station area at the site. No voes or BNAs were reported in this sample. Aroclor 1254 (1.08 ppb) was the only PCBs and/or Pesticides reported significantly above background in this sample. Arsenic (32 ppm), barium (220 ppm) and lead (110 ppm) were the only inorganics reported in significant concentrations in this sample. 12 I I , I I I I I I It I I I I I I I .. I TCE AREA COMPOSITE (GWSS04) A composite soil sample was collected in the TCE area at the site. No voes, BNAs or PCBs and/or Pesticides were reported in this sample. Arsenic (10 ppm) and lead (20 ppm) were the only inorganics reported in significant concentrations in this sample. LUMBER STACK SEDIMENT SAMPLE (GWSED0l) A sediment sample was collected adjacent the lumber stack area. No voes or BNAs were reported in this sample. Aroclor 1254 (0.30 ppb) was the only PCB and/or Pesticide reported above detection limit in this sample. Barium (27 ppm) and lead (27 ppm) were the only inorganics reported above detection limit in this sample. TCE SEDIMENT SAMPLE (GWSED02) A sediment sample was collected adjacent the TCE area. No voes, BNAs or PCBs and/or Pesticides were reported in this sample. Arsenic (9.8 ppm), barium (45 ppm), cadmium (160 ppm) and lead (20 ppm) were the only inorganics reported above detection limit in this sample. In conclusion, releases of hazardous contaminants have occurred to groundwater and soils on the site. Groundwater has releases of alpha BHC, delta BHC, gamma BHC (lindane), chloroethane, 1,2- dichloroethene (total), arsenic, beryllium, manganese and sodium. Soils on the site are contaminated with alpha BHC, delta BHC, gamma BHC (lindane), 4,4'-DDD, Aroclor 1254, arsenic, barium, calcium, chromium, cobalt, copper, iron, lead, magnesium, manganese and potassium. Sediments at the site appear to be contaminated with Aroclor 1254 and possibly arsenic, cadmium and lead. 13 I ~ I I I I I I I ' I I I I I I ' I I 5.0 RECOMMENDATIONS AND CONCLUSIONS Based on the analytical results of the sampling event at the Georgia Pacific Hardwood Sawmill site, the following areas have had environmental releases of hazardous contaminants that may be associated with the site: 0 0 0 0 0 0 0 groundwater in the green chain dip area is contaminated with alpha BHC, delta BHC, gamma BHC (Lindane), beryllium, and manganese. surface soils in the 4, 4-DDD, alpha BHC, barium, copper. lead, groundwater in the chloroethane, arsenic, green chain dip area are contaminated with beta BHC, delta BHC, gamma BHC (Lindane), magnesium, and manganese. TCE spill area and manganese. is contaminated with surface soils in the transformer station are contaminated with Aroclor 1254, arsenic, barium, chromium, and lead. surface soils in the TCE spill area are contaminated with arsenic, and lead. sediment in the ditch east of the sawmill complex is contaminated with Aroclor 1254 and lead. sediment in the ditch south of the TCE spill area is contaminated with arsenic, cadmium, and lead. Due to the fact that there is quantitative evidence of groundwater, soil, and sediment contamination around the facility and that several of the contaminants can be associated with the site activities, G&O is recommending that the Georgia-Pacific Hardwood Sawmill site move onto the next stage of the pre-remedial process. The Roanoke River, which supports recreation and fishing activities, is located immediately downstream from the site and Albemarle Sound is located less than 6 miles downstream from the probable point of entry. Also, wetlands are located around the perimeter of the facility as well as downstream along the river. No surface water samples were collected to characterize surface water in the area; however, samples were taken at two locations along drainage ditches surrounding the site. Since the ditches outfall to the river, contamination detected in the ditches indicates that migration of contaminants may be occurring. Further investigation is recommended in order to determine whether the site poses a threat to the environment or the public. 14 I ' I I I I I I I • I I I I I I I , I LIST OF REFERENCES FOR GEORGIA PACIFIC CORP. HARDWOOD SAi/MILL EPA I.D. NUMBER 000813592 1. Louis T. McAdams. (NUS). 1990. Letter to Mr. A.R. Hanke (EPA) regarding Screening Site Inspection, Phase I of the Georgia Pacific Corporation Hardwood Sawmill Site, August 20. 2. Potential Hazardous Waste Site Preliminary Assessment (EPA Form 2070- 12) for Georgia Pacific Corporation Hardwood Sawmill, Plymouth, North Carolina. Filed by Grover Nicholson, North Carolina Department of Human Resources, Solid and Hazardous Waste Management Branch, December 6, 1985. 3. EPA Hazardous Waste Permit Application (EPA Forms 3510-1 and 3510-3) for Georgia Pacific Corporation Hardwood Sawmill, Plymouth, North Carolina. Filed by H.S. Merscream, Senior Vice President, November 12, 1980. 4. Tim Beachum, Decatur Partnerships, telephone conversation with Louis McAdams, NUS Corporation, July 17, 1990. Subject: Facility ownership. 5. 0. W, Strickland, Head, Solid and Hazardous Waste Management Branch, Environmental Health Section, North Carolina Department Human Resources, Division of Health Services, letter to Gerald W. Tice, Senior Environmental Engineer for the South Division, Georgia Pacific Corporation, Augusta, Georgia, August 11, 1982. Subject: Change in RCRA status. 6. Jim Edwards, North Carolina Department of Human Resources, Hazardous Waste Branch, telephone conversation with Louis McAdams, NUS Corporation, June 20, 1990. Subject: Current facility status. 7. NUS Corporation Logbook No. F4-1719 for Georgia Pacific Corporation of facility Hardwood Sawmill, TDD No. F4-8909-89. Documentation reconnaissance, October 11 1989. 8. U.S. Geological Survey, 7.5-minute series Topographic Quadrangle Maps of North Carolina: Plymouth East 1954 (Photorevised 1974), Plymouth West 1979, Westover 1954, Woodard 1979, scale 1:24,000. 9. Greenhorne & O'Mara, Inc. 1991. Field notebooks for Georgia Pacific Hardwood Sawmill for documentation of facility reconnaissance. July 11. 10. RCRA Inspection Report for Georgia Pacific Sawmill, Plymouth, North Carolina, October 22, state file. Corporation Hardwood 1981; obtained from 11. National Archives and Records Administration Code of Federal Regulations Protection of Environment 40: Parts July 1, 1988 (Washington, D.C.: GPO, 1988). 120 to zgg. Revised I ' I I I I I I I • I I I I 0 D , I 12. Robert L. Metcalf, "Insect Control Technology," Kjrk-Othmer Encyclopedia of Chemical Technology. 3rd Edition, Volume 13 (New York: John Wiley & Sons, 1983). 13. Gerald W. Tice, Senior Environmental Engineer for the South Division- Georgia Pacific Corporation, Augusta, Georgia, letter to O. W. Strickland, Head, Solid and Hazardous Waste Management Branch, Environmental Health Section, North Carolina Department of Human Resources, Division of Health Services, November 30, 1981. Subject: Treatment process leak and leaking tank. 14. 0. W. Strickland, Head, Solid and Hazardous Waste Management Branch, Environmental Health Section, North Carolina Department of Human Resources, Division of Health Services, letter to Gerald W. Tice. Senior Environmental Engineer, South Division, Georgia Pacific Corporation, Plymouth, North Carolina, November 13, 1981. Subject: Remedial action for treatment process leakage planned. 15. Samuel Melver, NUS Corporation, telephone conversation with Sarah Winslow, Biologist for N.C. Division of Marine Fisheries, Subject: Fish caught in vicinity, January 25, 1990. 16. U.S. Department of Commerce, CJ imatic Atlas of the United States (Washington, D.C.: GPO, June 1968) Reprint: 1983, National Oceanic and Atmospheric Administration, pp. 43, 63 . 17. U.S. Department of Commerce, Rainfaj) Frequency At las pf the United States, Technical Paper No. 40 (Washington, D.C.: GPO. 1961), p.93. 18. Linda Aller, et al., DRASTIC: A Standardized System for Evaluating Ground Water Pollution Potential Using Hydrogeo]ogic Settings, EPA- 600/2-87-035 (Ada, Oklahoma: EPA, April 1987), pp. 270, 271. 19. Philip M. Brown, Chief Geologist, North Carolina Geologic Survey, North Carolina Geologic map, Department of Natural Resources, 1985. 20. U.S. Geological Survey, National Water S11mmary 1984; Hydrologic 21. Events, Selected Water Quality Trends and Ground-Water Resources, Water Supply Paper 2275 (1984), pp. 329-334. Richard Powers, Groundwater Section Division, telephone conversation with Brant Mccanless, and 20, 1990. Subject: Geology and Williamston, Martin County, North Carolina. Environmental Management, NUS Corporation, July 19 aquifer information for 22. Perry F. Nelson, Geology and Ground-Water Resources of the swanquarter Area North Carolina, Ground-Water Bulletin Number 4 (Raleigh, North Carolina, 1964), pp. 54, 55, 76, 77. 23. Allen Spencer, Bell Grey Well Drilling, telephone Brant Mccanless, NUS Corporation, February 22, 1990. and water levels in Plymouth, North Carolina. conversation with Subject: Geology I I I I I I I I I I I I I n r 24. R. Allan Freeze and John A. Cherry, Groundwater (Englewood Cliffs, N.J.: Prentice-Hall, Inc., 1979), p.29. 25. Soil Conservation Service. Soi 1 Survey of Washington County North Carol jna, United States Department of Agriculture, Soil Conservation Service, December 1981. 26. North Carolina Department of Transportation, llashington County, North Carolina, Revised, January 1, 1990. 27. Department of Commerce, 1990 Census Information: Table 6. Household, Family and Group Quarters Characteristics. 28. Mendoza, Irene (G&O) 1991. Population and \later Supply Computations, December 5. 29. North Carolina Department of Human Resources, Environmental Health Section, \later Supply Branch, Alphabetic Listing of Public \/ell Systems within \lashington County, Report No. 110415-ALPHA IIANG July 10, 1990. 30. Mr. Long, Director, \lashington System, Louis McAdams, NUS Corporation, July 19, water service in the Plymouth area. telephone conversation with 1990. Subject: Extent of 31. DeRosa, Pat (NC Superfund Branch). 1989. Memo (and attachments) to File concerning Habitats of Federally Listed Endangered Species in North Carolina, Division of Health Services, Raleigh, NC, May 18. 32. North Carolina Natural Heritage Program Element List of \lashing ton County, North Carolina, November 22, 1989. 33. U.S. Environmental Protection Agency, Environmental Services Division, Environmental Compliance Branch Standard Operating Procedures and Quality Assurance Manual. Athens, Georgia, February 1, 1991. 34. U.S. Environmental Protection Agency, Office of Drinking \later Regulations and Health Advisories. November 1990. 35. Division of Environmental Management, Raleigh, North Carolina, NCDEHNR, Classification and Water Quality Standards Assigned to the Waters of the Roanoke River Basin November 1, 1990. I .. I I I I I I I • I a I m I, I I r I . APPENDIX A MAPS ' PI-IOTOGRAPIIS, AND rrAB 1 I I I I I I I I ,._ n R u I I WASHINGTON COUNTY, N.C. N t ,._ B"SO' s ' \l c, c.,~., ill! c. '•, ' , I ~ ' ~ - GEORGIA PACIFIC CORPORATION HARDWOOD SAWMILL PLYMOUTH, NC FIGURE 1 ,r;a (1161/lllRS • UCIIIIICIS • l'IIUtAS • SCll-llSIS • SUl'l'ITOIIS • l'><0I0CIIU.i .. 1111,sa GREENHORNE & O'MARA, INC. 9001 EDMONSTON ROAD. GREENBB..T. MARYLAND 20no ! 3011 982-2BOO ,.,.,,P•••~ .,.., .• ,. • .,,.,., •• ,, .. ,,..,co,.,_.,,,..._ '"'l•~""'"'" ,,.,,,_,,,., ,., '., .. ~,, ~,., ... ,,, ......... ~~•~ ..... ,,o;,, ............. , ,...,,,. .... ," SITE LOCATION NCD 000813592 I SOURCE: North Carolina Department of Transportation, County Road i,taps, 1990. I, I le I I I I I n IP D I I I I r I SOURCE : USGS Topographic Map, Westover & Plymouth East, N.C. GEORGIA PACIFIC CORPORATION HARDWOOD SAWMILL PLYMOUTH, NC SCALE 1· = 2000' CONTOUR INTERVAL 5 FEET GREENHORNE & O'MARA. INC. 9001 E~STON ROAD. GREENBELT, MARYlAND 2DTT0 ( 3111 982. 2800 FIGURE 2a SITE LOCATION MAP NCD 000813592 -------- flow • -- ROANOKE ,----------------- 1 I I I Burner I GWOl ® ( background I liiil RI VER Temporary Stacking Area - flow .. -- . \ \ \ \ \ \ Green Chain I I Conveyor System I I /sso, -r , a ~~ i , Former location otHr--------i g ~ old asphalt plant -I TCE Spill I Shed ---.,.. Area GW-03 ___ '-I 1 --------- I I SS~4<1> ) 'i------------I L '... ____ J I, ----------, ___ ----.....:,-c_c_ __ -l __ Di_\_e_h _ SED02 GEORGIA PACIFIC CORPORATION HARDWOOD SAWMILL NCO 000813592 PLYMOUTH, NC [MGM((~S • IRCfllHCIS • l'\UO<(RS • SCll'fllS!S • S~V!TCA~.° ""'010(;U, .. •(UIS!S GREENHORNE & O'MARA, INC. 9001 EDr,'lQ\/STOr~ ROAD. GREENBELT, MARYLArJD :-0770 13011 9'82.28C() .i. .. ~,s ... ::l_!•Hh!O C.••,tC•ll• -•CUl'"l""t• ·••ot"•i• (1,1.t,"O•T ••• ,.,a,., •• ,;irfllS,,l,CJ~O o,c ... o,,,aO( ... ,.a,,1,c.,, ..C••oc, ..... u .. g,h .. •• '\• .. ,.us10,,•ua •• SITE LAYOUT AND SAMPLING POINTS NOT TO SCALE I FIGURE 2b - I I I I I I I It I I I I I I I , I Photo 1 -Location of background groundwater sample (G\101) and background surface soil sample (SSOl). Photo 2 -Location of surface soil composite sample (SSOZ). I .. I I I I I I I It I I I I I I I , I """1fl'l~"!~~j[ ~~--s ~.,,.,, ' ,I ' " .. lumber mill. the former '1·;,( C )J _i::,j, 'lled. reportedly spi I • ;:::-···. . . : .. ;,.,.,.,;ijj ·. '-. . ,' ,·4• _.;;,.- A~ --~. . ' ,/ :, 'S:, ,,~, ' I '-- • ~-_" I, ~ ' , . ~z·-_ ·-~.:-, -· .. '~,,. . -.,, .: ~ -' --·. in area w I I I I I I I It I I I I I I I , I Photo 5 -Location of suspected _green chain dip area of the former lumber mill. Photo 6 -Old belts of the green chain system. I I I I I I I I I I I I I I , I Photo 7 -Former area where lumber was temporarily stacked when it came off of the green chain. -Photo 8 -Stacks to the old boiler room which heated the kilns and incinerated sawdust. Machine r9om is on the right. ----- -- -- ---- TABLE 2A SUMMARY OF CHEMICAL ANALYSES FOR THE GEORGIA-PACIFIC HARDWOOD SAWMILL SITE NCD000813592 SAMPLE IDENTIFICATION Sample Collection Information and Parameters Date Collected Laboratory Well Water Depth (Feet) G&O Sample ID No. EPA Case No. Case No. Back- ground Ground- water 7/11/91 !EA 3.5 GUGU01 GN180 1041-037 Green Chain & Dip Area Ground- water 7 /11/91 !EA 5 .0 GWGW02 GN181 1041-037 Physical Waste State Gas Gas Gas Gas Liquid Liquid Liquid Liquid Liquid Liquid Liquid Liquid Liquid Liquid Characteristics* Category Compounds Detected VOLATILE ORGANICS Matrix A,D,G, I DCC A,D,G, I DCC A,D,G, I DCC A,D,G, I DCC A,D,H, I SOL E,H, I, A SOL A,H, I SOL A,D,G, I SOL A,D,H,G SOL A,D,G SOL A,D SOL A,D,G · SOL A,E,G SOL Level ¾ Moisture Concentration Units chloromethane bromomethane vinyl chloride chloroethane methylene chloride acetone carbon disulfide 1,1-dichloroethene 1,1-dichloroethane 1,2-dichloroethene chloroform 1,2-~ichLOrOethane 2-butanone (MEK) (total) A,D SOL 1,1,1-trichloroethane Water Low 100 ug/l [10U] Water Low 100 ug/l - Back- ground Surface Soil 7/11/91 !EA NA GWSS01 GN182 1041-037 Soil Low 18 ug/kg - - Green Chain & Dip Area Surface Soil Composite 7 /11/91 !EA NA GWSS02 GN183 1041-037 Soil Low 19 ug/kg - Trip Blank 7 /11/91 !EA NA GWTB01 GN186 1041-037 Water Low 100 ug/L --.. TCE Spill Area Groundwater 7 /11/91 !EA 5.0 GWGW03 GN187 1041-037 Water Low 100 ug/l 99011 19J - ----- --- - -... -------.. II!!!! TABLE 2A SUMMARY OF CHEMICAL ANALYSES FOR THE GEORGIA-PACIFIC HARDWOOD SAWHILL SITE NCD000813592 SAMPLE IDENTIFICATION Green Green Back.-Chain & Back-Chain & TCE ground Dip Area ground Dip Area Spill Sample Collection Information Ground-Ground-Surface Surface Soil Trip Area and Parameters water water Soil Composite Blank Groundwater Physical Uaste State Characteristics• Category VOLATILE ORGANICS (CONT.) Liquid A,D SOL carbon tetrachloride Liquid A,0,G SOL vinyl acetate Liquid A,D occ bromodichloromethane Liquid A,D,G SOL 1,2-dichloropropane Liquid A,D,G SOL cis-1,3-dichloropropene Liquid A,D,G,B SOL trichloroethene Liquid A,D occ dibromochloromethane Liquid A,D SOL 1,1,2-trichloroethane Liquid A,G SOL benzene Liquid A,D,G SOL trans-1,3-dichloropropene Liquid A,D SOL bromoform Liquid A,E,G SOL 4-methyl-2-pentanone p A,E,G SOL 2-hexanone Liquid A,D SOL tetrachloroethene Liquid A,G,E SOL toluene Liquid A,D,E SOL 1,1,2,2-tetrachloroethane Liquid A,D,G SOL chlorobenzene Liquid A,G SOL ethyl benzene Liquid A,D,G occ styrene Liquid A,G SOL xylenes (total) Tentatively Identified Compounds (Total) Unknown 72JN Substituted aromatic 63JN Substituted benzene 12JN ------ Physical Waste State Characteristics• Category S, thick1 A,B,E ace Liquid A,D,B ace Liquid A,D,B ace Liquid A,D,H SOL Sol id A,D,H ace Liquid A,D,H SOL Liquid A,D,H ace Liquid A,B ace A,D ace Liquid A,B ace A ace Sol id A,D ace Liquid A,D ace Liquid A,D ace Sol id A,D ace Sol id A,B ace Sol id A ace A,D ace Liquid A,D ace Liquid A,D ace Sol id A ace Sol id A,D ace Liquid A,D,B ace - - -----TABLE 2A SUMMARY OF CHEMICAL ANALYSES FOR THE GEORGIA-PACIFIC HARDWOOD SAWMILL SITE NC 0000813 592 SAMPLE IDENTIFICATION Green Back-Chain & ground Dip Area Sample Collection Information Ground-Ground- and Parameters water water SEHIVOLATILE ORGANICS Matrix \.later I.later Level Low Low % Moisture 100 100 Concentration Units ug/l ug/l phenol bis(2-chloroethyl)ether 2-chlorophenol 1,3-dichlorobenzene 1,4-dichlorobenzene benzyt alcohol 1,2-dichlorobenzene 2-methylphenol bis(2-chloroisopropyl)ether 4-methylphenol [1DUJ n-nitroso-di-n-dipropylamine hexachloroethane nitrobenzene isophorone 2-ni trophenol 2,4-dimethylphenol benzoic acid bis(2-chloroethoxy)methane 2,4-dichlorophenol 1,2,4-trichlorobenzene naphthalene [10UJ 4-chloroani line hexachlorobutadiene -- - Green Back-Chain & ground Dip Area Surface Surface Soi t Soil Composite Soil Soil Low Low 18 19 ug/kg ug/kg - Trip Blank NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA --.. TCE Spi LL Area Groundwater Water Low 100 ug/l /RE [1JJ/[1JJ - --.. ---- - -... --- -- - -.. -TABLE 2A SUMMARY OF CHEMICAL ANALYSES FOR THE GEORGIA-PACIFIC HARDWOOD SAWMILL SITE NCD000813592 SAMPLE IDENTIFICATION Green Green Back-Chain & Back-Chain & TCE ground Dip Area ground Dip Area Spill Sample Collection Information Ground-Ground-Surface Surface Soil Trip Area and Parameters water water Soil Composite Blank Groundwater Physical Waste State Characteristics• Category SEMIVOLATILE ORGANICS (CONT.) Sol id A,O occ 4-chloro-3-methylphenol NA Liquid A,O occ 2-methylnaphthalene NA Liquid A,0,8 occ hexachlorocyclopentadiene NA Solid A,O occ 2,4,6-trichlorophenol NA Sol id A,D occ 2,4,5-trichlorophenol NA Liquid A,D occ 2-chloronaphthalene NA Sol id A,D occ 2-nitroanil ine NA Liquid A,D occ dimethylphthalate NA Sol id A,D occ acenaphthylene NA Solid A,D occ 2,6-dinitrotoluene NA Sol id A,D occ 3-nitroaniline NA Sol id A,D occ acenaphthene NA Sol id A,D,G occ 2,4-dinitrophenol NA Solid A,D occ 4-nitrophenol NA Sol id A,D occ dibenzofuran NA Solid A,D occ 2,4-dinitrotoluene NA Liquid A,D occ diethylphthalate [2JJ NA [2JJ/[2J] A,D occ 4-chlorophenyl-Phenylether NA Sol id A,D occ fluorene NA Sol id A,D,E occ 4-nitroanil ine NA Sol id A,D occ 4,6-dinitro-2-methylphenol NA Sol id A,D occ n-nitrosodiphenylamine NA Liquid A,D occ 4-bromophenyl-phenylether NA Sol id A,D occ hexachlorobcnzene NA Sol id A,D occ pentachlorophenol [970U] [690JJ NA Sol id A,D occ phenanthrene NA ---- -- -- -... - ------.. l!!!l!!l!I TABLE 2A SUMMARY OF CHEMICAL ANALYSES FOR THE GEORGIA-PACIFIC HARDWOOD SAYMJLL SITE NC0000813592 SAMPLE IDENTIFICATION Green Green Back-Chain & Back-Chain & TCE ground Dip Area ground Dip Area Spill Sample Collection Information Ground-Ground-Surface Surface Soil Trip Area and Parameters water water Soil Composite Blank Groundwater. Physical Uaste State Characteristics• Category SEHIVOLATILE ORGANICS (CONT.) Sol id A; 0 occ anthracene NA Liquid A,D DCC di-n-butylphthalate [400U] NA Sol id A,D occ fluoranthene NA Sol id A,O ace pyrene [10U] [400U] NA [1JJ Liquid A,D ace butylbenzylphthalate NA A,D ace 3,3-dichlorobenzidine NA Sol id A,D ace benzo[a]anthracene NA Sol id A,D ace chrysene [400UJ [100JJ NA Liquid A,D ace bis(2-ethylhexyl)phthalate NA Liquid A,O ace di-n-octylphthalate NA Sol id A,0 ace benzo[b]fluoranthene [400U] . -NA Solid A,O CCC benzo[k]fluoranthene [400U] NA Sol id A,D,K,L ace benzo[a]pyrene [400U] [100J] NA Solid A,O ace indeno(1,2,3-cd]pyrene NA Sol id A,0 ace dibenz(a,h]anthracene NA Sol id A,D ace benzo[g,h,i]perylene NA Tentatively Identified NA Compounds (Total) NA Unknown (Total) NA 3BJN 370BJN NA Unknown 225JN 77JN ·11,090JN 18590JN NA 169JN substituted benzoic acid 9JN NA substituted naphthalene 410JN NA 2-propanol,1-(2-methoxy-l-m) NA 6JN substituted propanol NA 7JN substituted bi cyclo[2. 2. 1 ]he NA 6JN --.. --- -- -.. ----- - - fr l!l!!!I TABLE 2A SUNHARY OF CHEMICAL ANALYSES FOR THE GEORGIA-PACIFIC HARDWOOD SAWHILL SITE NC0000813592 SAMPLE IDENTIFICATION Green Green Back-Chain & Back-Chain & TCE ground Dip Area ground Dip Area Spill Sample Collection Information Ground-Ground-Surface Surface Soil Trip Area and Parameters water water Soil Composite Blank Groundwater PEST IC lDES/PCBs Matrix Water Water Soil Soil NA Water level Low Low Low Low NA Low Physical Waste X Moisture 100 100 18 19 NA 100 State Characteristics* Category Concentration Units ug/l ug/l ug/kg ug/kg NA ug/l /DL Solid A,D PSD alpha BHC [0.0SU] 0.12 [2.1U] 640XE/470 NA Sol id A,D PSD beta BHC [0.05U] [0.045 J] [2.1U] NA Sol id A,0 PSD delta BHC [0.05U] 0.13 [2.1U] 560XE/480 NA Sol id A,D PS0 gamma BHC (Lindane} [0.0SU] 0,32 [2,1U] 1200XE/98G NA Sol id A,D PSD Heptachlor 0,31 NA Sol id A,D PSD Aldrin NA Sol id A,D PSD Heptachlor epoxide NA Sot id A,D PSD Endosul fan NA Sol id A,O,E PSD Dieldrin NA Sol id A,D PSD 4,4'-DDE NA Sot id A,D PSD Endrin NA Sol id A,D PSD Endosul fan II NA Sol id A,D PSD .4,4'-DDD [4,0U] 170(f[150JD] NA Solid A,D PS0 Endosul fan sut fate NA Sot id A,D PSD 4,4'-DDT NA Sol id A,D PSD Hethoxychlor (Mari ate) NA Sol id A,0 PS0 Endrin ketone NA Sol id A,D PSD alpha Chlordane 0,28 NA Sol id A,D PSD gamma Chlordane NA Sot id A,D PSD Toxaphene [210U] [450XJP]/10000U] NA m I , I TABLE 2A GEORGIA-PACIFIC NCD 000 813 592 I INORGANICS WATER NCMCL (PPB) WATER MCL (PPB) GWGWOl (PPB) GWGW02 (PPB) GWGW03 (PPB) I ALUMINUM 300000J 690000J 20000J ANTIMONY 10/5 42UR 42UR 42UR ARSENIC 50 2UJ GUJ 43J I BARIUM 1000 5000 lOOOJ 2900J 960J BERYLLIUM 1 2J 12J lUR CADMIUM 5 5 4UJ 4UJ 4UR I CALCIUM 130000J 170000J 210000J CHROMIUM 50 100 340J 740J 81J - COBALT 76J lOOJ llJ COPPER 1000 1300 llOJ 270J 31J I IRON 300 310000J 340000J 71000J LEAD 50 50 270J 170J 140J MAGNESIUM 25000J 40000J 28000J WAN GANE SE 50 1300J GOOOJ 4300J ERCURY 1.1 2 1. 7J 1. SJ 0.20UR ICKEL 150 100 150J 420J 52J POTASSIUM 20000J 49000J 36000J I SELENIUM 10 50 lUR 20UJ 2UJ SILVER 50 SUR SUR SUR SODIUM 8000J 6500J 96000J I THALLIUM 2/1 2UJ 2UJ 2UJ VANADIUM 540J 920J 42J ZINC 5000 330J 940J 320J I CYANIDE 154 200 u u u NOTES: I 1) NA -NOT ANALYZED 2 ) N -PRESENCE OF CONTAMINANT PRESUMED 3) J -CONCENTRA'rI ON ESTIMATED I 4 ) u -NON-DETECT 5) R -DATA UNUSABLE 6) B -CONTAMINANT FOUND IN THE ASSOCIATED BLANK I 7 ) NCMCL -NORTH CAROLINA MAXIMUM CONTAMINANT LEVEL 8 ) MCL -FEDERAL MAXIMUM CONTAMINANT LEVEL I .. I D I , I I INORGANICS SOILS NATURAL RANGE (PPM) TABLE 2A GEORGIA-PACIFIC NCD 000 813 592 GWSSOl (PPM) GWSS02 (PPM) ------------------------------------------I ALUMINUM 0.7->10% 7000 5600 ANTIMONY <1-8.8 :!OUR 20UR ARSENIC <0.1-73 3U 3U I BARIUM 10-1500 29 320 BERYLLIUM <1-7 0.26 0.34 CADMIUM 0.01-0.7 lU lU I CALCIUM 0.01-20% 580 79000 CHROMIUM 1-1000 8.1 8.3 COBALT <0.3-70 1. 3U 5.3 COPPER <1-700 3.0 23 I IRON 0.01->10% 6900 5600 LEAD <10-300 5.8 33 MAGNESIUM 0.005-5% 380 3600 WANGANESE <2-7000 42 850 ERCURY 0.01-3.4 0.29U 0.28U ICKEL <3-700 4.1 9.8 I POTASSIUM 0.005-3.7% 470 1800 SELENIUM <0.1-3.9 0.26U lU SILVER 0.01-5 1. 31J 1. 3U SODIUM 0.05-5% 250U 480U I THALLIUM 0.53U 0.53U VANADIUM <7-500 13 11 ZINC <5-2900 29 81 I CYANIDE u u NOTES: I 1) NA -NOT ANALYZED 2) N -PRESENCE OF CONTAMINANT PRESU 3) J -CONCENTRATION ESTIMATED I 4 ) u -NON-DETECT 5) B -CONTAMINANT FOUND IN ASSOCIAT 6 ) R -DATA UNUSABLE I I .. I -----I!!!!!! Physical Waste State Characteristics* Category Gas A,D,G, I CCC Gas A.D.G. I CCC Gas A,D,G, I CCC Gas A,D,G, I CCC Liquid A.D,H, I SOL Liquid E,H, l,A SOL Liquid A,H, I SOL Liquid A,D,G. I SOL Liquid A,D,H,G SOL Liquid A,D,G SOL Liquid A,D SOL Liquid A,D,G SOL Liquid A,E,G SOL Liquid A,O SOL !!111!1 liiii liiiill • - TABLE 2B SUMMARY OF CHEMICAL ANALYSES FOR THE GEORGIA-PACIFIC HARDWOOD SAWMILL SITE NC0000813592 SAMPLE IDENTIFICATION -- Analyzed at the North Carolina State Laboratory of Public Health Sample Collection Information and Parameters Date Collected Laboratory Well Depth (Feet) G&O Semple IO No. NCDEHNR No. Field No. Compounds Detected VOLATILE ORGANICS Matrix Concentration Units chloromethane bromomethane vinyl chloride chloroethane methylene chloride acetone carbon disulfide 1,1-dichloroethene 1,1-dichloroethane 1,2-dichloroethene (total) chloroform 1,2-dichloroethane 2-butanone (MEK) 1,1,1-trichloroethane Trip Blank 7/9/91 SLPH NA GWTB02 15010 912625 15010 Water ug/l Trace Transformer Station TCE Lumber Surface Surface Stacks Soil Soil Ditch 7 /9/91 7/9/91 7 /9/91 SLPH SLPH SLPH NA NA NA GWSS03 GWSS04 GWSED01 15011 15012 15013 912626 912627 912628 15011 15012 15013 Soil Soil Soil ug/kg ug/kg ug/kg - - --r TCE Down- gradient Ditch 7/9/91 SLPH NA GUSED02 15014 912629 15014 Soil ug/k.g ----- - Physical Waste State Characteristics* Category Liquid A,D SOL Liquid A,D,G SOL Liquid A,D ace Liquid A,D,G SOL Liquid A,D,G SOL Liquid A,0,G,B SOL Liquid A,D CCC Liquid A,D SOL Liquid A,G SOL Liquid A,D,G SOL Liquid A,D SO!... Liquid A,E,G SOL p A,E,G SOL Liquid A,D SOL Liquid A,G,E SOL Liquid A,D,E SOL Liquid A,D,G SOL Liquid A,G SOL Liquid A,D,G CCC Liquid A,G SDL -l!!!!!!!l!!I l!!!!I liiiiiil TABLE 2B SUMMARY OF CHEMICAL ANALYSES FOR THE GEORGIA-PACIFIC HARDWOOD SAWHILL SITE NC0000813592 SAMPLE IDENTIFICATION - Analyzed at the North Carolina State Laboratory of Public Health Transformer Station TCE Lumber Semple Collection Information Trip Surface Surface Stacks and Parameters Blank Soil Soil Ditch VOLATILE ORGANICS (CONT.) carbon tetrachloride vinyl acetate bromodichloromethane 1,2-dichloropropane cis-1,3-dichloropropene trichloroethene dibromochloromethane 1,1,2-trichloroethane benzene trans-1,3-dichloropropene b;-c,;riuiur·m 4-methyl-2-pentanone 2-hexanone tetrachloroethene toluene 1,1,2,2-tetrachloroethane chlorobenzene ethyl benzene styrene xylenes (total) tetrachydrofuran Trace -- --r - TCE Down- gradient Ditch -.. !!!!!!I 1!!!119 1111:.'1 State Characteristics* Category S,thick1 A,B,E occ Liquid A,0,8 occ Liquid A,O,B occ Liquid A,O,H SOL Sol id A,0,H occ Liquid A,O,H SOL Liquid A,O,H DCC Liquid A,B occ A,D occ Liquid A,B DCC A occ Sol id A,D occ Liquid A,D occ Liquid A,D occ Sol id A,D occ Sol id A,B DCC Solid A occ A,O occ Liquid A,D occ Liquid A,O occ Sol id A occ Sol id A,D occ Liquid A,D,B occ == liiiil ., -TABLE 28 SUMMARY OF CHEMICAL ANALYSES FOR THE GEORGIA-PACIFIC HARDWOOD SAWHILL SITE NC0000813592 SAMPLE IDENTIFICATION -- Analyzed at the North Carolina State Laboratory of Public Health Transformer Station TCE Lumber Sample Collection Information Trip Surface Surface Stacks and Parameters Blank Soil Soil Ditch Matrix Water Soil Soil Soil Concentration Units ug/kg ug/kg ug/kg phenol bis(2-chloroethyl)ether 2-chlorophenol 1,3-dichlorobenzene 1,4-dichlorobenzene benzyl alcohol 1,2-dichtorobenzene 2-methylphenol bis ( 2-ch loroi sopro·pyl )ether 4-methylphenol n-nitroso~di-n-diproµylaminP. hexachloroethane nitrobenzene i sophorone 2-nitrophenol 2,4-dimethylphenol benzoic acid bis(2-chloroethoxy)methane 2,4-dichlorophenol 1,2,4-trichlorobenzene naphthalene 4-chloroani line hexachlorobutadiene - ------ TCE Down- gradient Ditch Soil ug/kg ----- - Physical lJaste State Characteristics• Category Sol id A,D CCC Liquid A,D CCC Liquid A,0,8 CCC Sol id A,D CCC Sol id A,D CCC Liquid A,D CCC Sol id A,D CCC Liquid A,D CCC Sol id A,D CCC Sol id A,D CCC Sol id A,D CCC Sol id A,D CCC Sol id A,D,G CCC Sol id A,D CCC Sol id A,D CCC Sol id A,D CCC Liquid A,D CCC A,D CCC Sol id A,D CCC Sol id A,D,E CCC Sol id A,D CCC Solid A,D CCC Liquid A,D CCC Sol id A,D CCC Sol id A,D CCC Sol id A,D CCC - - - --TABLE 28 SUMMARY OF CHEMICAL ANALYSES FOR THE GEORGIA-PACIFIC HARDWOOD SAWHILL SITE NCD000813592 SAMPLE IDENTIFICATION -- Analyzed at the North Carolina State Laboratory of Public Health Sample Collection Information and Parameters SEMIVOLATILE ORGANICS (CONT.) 4-chloro-3-methylphenol 2-methylnaphthalene hexachlorocyclopentadiene 2,4,6-trichlorophenol 2,4,5-trichlorophenol 2-chloronaphthalene 2-nitroaniline dimethylphthalate acenaphthylene 2,6-dinitrotoluene 3-nitroanil ine acenaphthene 2,4-dinitroµhenol 4-ni trophenol dibenzofuran 2,4-dinitrotoluene diethylphthalate 4-chlorophenyl-Phenylether fluorene 4-nitroaniline 4,6-dinitro-2-methylphenol n-nitrosodiphenylamine 4-bromophenyl-phenylether hexachlorobenzene pentachlorophenol phenanthrene Trip Blank Transformer Station Surface Soil TCE Surface Soil Lumber Stacks Ditch - - TCE Down- gradient Ditch --r l!II!!!!! ------ Physical Waste State Characteristics* Category Solid A,D DCC Liquid A,D DCC Sol id A,D ace Solid A,D ace Liquid A,D ace A,D ace Sol id A,D ace Sol id A,D ace Liquid A,D ace Liquid A,D ace Solid A,D ace Sol id A,D ace Solid A,D,K,L ace Sol id A,D ace Sol id A,D ace Sol id A,D ace - - - -.. -TABLE 28 SUMMARY OF CHEMICAL ANALYSES FOR THE GEORGIA-PACIFIC HARDWOOD SAWMILL SITE NC0000813592 SAMPLE IDENTIFICATION - Analyzed at the North Carolina State Laboratory of Public Health Sample Collection Information and Parameters SEHIVOLATILE ORGANICS (CONT.) anthracene di-n-butylphthalate fluoranthene pyrene butylbenzylphthalate 3,3-dichlorobenzidine benzo[a)anthracene chrysene bis(2-ethylhexyl)phthalate di-n-octylphthalate benzo[b]fluoranthene b~nzo[k]fluoranthene benzo[a)pyrene indeno[1,2,3-cd]pyrene dibenz[a,h]anthracene benzo(g,h,i]perylene Trip Blank Transformer Station Surface Soil TCE Surface Soil - Lumber Stacks Ditch - - TCE Down- gradient Ditch -!11!!1!! -.. - - --- - -.. - -- -- - -r !I!! TABLE 2B SUMMARY OF CHEMICAL ANALYSES FOR THE GEORGIA-PACIFIC HARDWOOD SAWMILL SITE NC0000813592 SAMPLE IDENTIFICATION Analyzed at the North Carolina State Laboratory of Public Health Transformer TCE Station TCE Lumber Down- Sample Collection In format ion Trip Surface Surface Stacks gradient and Parameters Blank Soil Soil Ditch Ditch PESTICIDES/PCBs Matrix NA Soil Soil Soil Soil State Characteristics* Category Concentration Units NA mg/kg mg/kg mg/kg mg/kg Solid A,D PSD alpha BHC NA NA NA NA NA Sol id A,D PSD beta BHC NA NA NA NA NA Sol id A,D PSD delta BHC NA NA NA NA NA Sol id A,D PSD gamma BHC (L indane) NA <0.40 <0.40 <0.40 <0.40 Solid A,D PSD Heptachlor NA NA NA NA NA Solid A,D PSD Aldrin NA NA NA NA NA Sol id A,D PSD Heptachlor epoxide NA NA NA NA NA Solid A,D PSD Endosul fan NA NA NA NA NA Sol id A,D,E PSD Dieldrin NA NA NA NA NA Solid A,D PSD 4,4'-DDE NA NA NA. ~.~ "" Sol id A,D PSD Endrin NA <0.10 <0.10 <0.10 <0.10 Sol id A,D PSD Endosul fan II NA NA NA NA NA Sol id A,D PSD 4,4' -DOD NA NA NA NA NA Sol id A,D PSD Endosul fan sulfate NA NA NA NA NA Sol id A,D PSD 4,4'-DDT NA NA NA NA NA Sol id A,D PSD Methoxychlor (Mariate) NA <1.0 <1.0 <1.0 <1.0 Solid A,D PSD Endrin ketone NA NA NA NA NA Solid A,D PSD alpha Chlordane NA NA NA NA NA Sol id A,D PSD gamma Chlordane NA NA NA NA NA Solid A,D PSD Toxaphene NA <2.0 <2.0 <2.0 <2.0 ----- Physical Waste State Characteristics* Category Liquid A,0 occ Liquid A,0 occ Liquid A,D occ Liquid A,D occ Liquid A,D occ Liquid A,D occ Liquid A,0 ace -- --.. -TABLE 28 SUMMARY OF CHEMICAL ANALYSES FOR THE GEORGIA-PACIFIC HARDWOOD SAWMILL SITE NC0000813592 SAMPLE IDENTIFICATION -- Analyzed at the North Carolina State Laboratory of Public Health Sample Collection Information and Parameters PEST IC IDES/PCBS (CONT.} Aroclor 1016 Aroclor 1221 Aroclor 1232 Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260 2,4-0 2,4,5-TP Trip Blank NA NA NA NA NA NA NA NA NA Transformer Station Surface Soil NA NA NA NA NA 1.08* NA <0.10. <0.10 TCE Surface Soil NA NA NA NA NA <0.10 NA <0.10 <0.10 Lumber Stacks Ditch NA NA NA NA NA 0.30* NA <0.10 <0.10 - - TCE Down- gradient Ditch NA NA NA NA NA <O 10 NA <0.10 <0.10 -l!!!l!!I ------ State Characteristics* Category Sol id A,O MES Sol id A,D MES Sol id A,O MES Sol id A,D MES Sol id A,D MES Sol id A,D MES Sol id D MES Sol id A,O MES Sol id A,D HES Solid A,0 MES Sol id A,O MES Sol id A,0 MES Solid A,D MES Sol id A,D MES Liquid A,O MES Solid A,O MES Sol id 0 MES Sol id A,0 MES Sol id A,D HES Sol id D MES Sol id A,O MES ----,,. -TABLE 2B SUMMARY OF CHEMICAL ANALYSES FOR THE GEORGIA-PACIFIC HARDWOOD SAWMILL SITE NC0000813592 SAMPLE IDENTIFICATION --- - Analyzed at the North Carolina State Laboratory of Public Health Transformer TCE Station TCE Lumber Down- Sample Collection Information Trip Surface Surface Stacks gradient and Parameters Blank Soil Soil Ditch Ditch ANALYTE DETECTED Matrix NA Soil Soil Soil Soil Concentration Units NA mg/kg/mg/l mg/kg/mg/l mg/kg/mg/l mg/kg/mg/l Total/TCLP Total/TCLP Total/TCLP Total/TCLP aluminum NA NA NA NA NA antimony NA NA NA NA NA arsenic NA 32*/0.07 10•;0.02 <2.0/<0.01 9.8*/0.05 barium NA 220"'"/1 .00 30/0. 58 27/0.42 45/0.62 beryllium NA NA NA NA NA cadmium NA <30/0.08 <20/<0.08 <15/<0.08 160*/<0.08 calcium NA NA NA NA NA chromium NA 40*/<0.10 <20/<0.10 <20/<0.10 <20/<0.10 cobalt NA NA NA NA NA copper NA NA NA NA NA iron NA ~-·· nM iiA. NA lead NA 110*/<0.50 20*/<0. 50 27*/<0.50 20*/<0.50 magnesium NA NA NA NA NA manganese NA NA NA NA NA mercury NA <0.09/<0.02 <0.09/<0.02 <0.1/<0.02 <0.1/<0.02 nickel NA NA NA NA NA potassium NA NA NA NA NA selenium NA <1.7/<0.005 <1.0/<0.005 <1.0/<0.005 <1.0/<0.005 silver NA <30/<0.10 <20/<0.10 <20/<0.10 <20/<0. 10 sodium NA NA NA NA NA thallium NA NA NA NA NA -l!!!e.9 - -- Physical Waste State Characteristics* Category Sol id A,D MES Sol id A,D MES Sol id A ICC ----.. -TABLE 28 SUMMARY OF CHEMICAL ANALYSES FOR THE GEORGIA-PACIFIC HARDWOOD SAWMILL SITE NCDOOOB13592 SAMPLE IDENTIFICATION -- Analyzed at the North Carolina State Laboratory of Public Health Sample Collection Information and Parameters ANALYTE DETECTED (CONT.) vanadium zinc cyanide NA Not Analyzed Trip Blank NA NA NA Transformer Station Surface Soil NA NA NA * Concentrations significant, considered to be a release TCE Surface Soil NA NA NA Lumber Stacks Ditch NA NA NA - - TCE Down- gradient Ditch NA NA NA ----- -.. --- COMPOUND QUALIFIERS u J UJ C B --- - • - DEFINITION Indicates compound was analyzed for but not detected. Indicates an estimated value. Quantitation limit is estimated due to a quality control (QC) protocol. This flag applies to pesticide results where the identification has been confirmed by GC/MS. Single component pesticides ~10 ng/uL in thj final extract shall be confirmed by GC/MS. This flag is used when the compound is found in the associated blank as ·well as in the sample. It indicates possible/probable blank contamination and warns the data user to take appropriate action. ---- INTERPRETATION Compound was not detected at or above the CRDL. Com1>ound value may be semi- quantitative. Compound was not detected if value is at CRDL, e.g., 100 UJ. If a value is reported with a UJ above CRDL and it is <Sx blank concentration (lOx for common laboratory artifacts), the compound is detected but may be a laboratory artifac and not attributable to the sample. Compound was confirmed by GC/MS and is quantitative. Use pesticide/PCB listed value. Compound value may be semi- quantitative if it is <Sx the blank concentration (<lOx the blank concentrations for common laboratory artifacts: phthalates, methylene chloride, acetone, toluene, 2- butanone). !!!!!I ---- COMPOUND QUALIFIERS E D A R X ANALYTE QUALIFIERS E E s s R N .. -• - DEFINITION This flag identifies compounds whose concentrations exceed the calibration range of the GC/HS instrument for the specific analysis. This flag will llll..l apply to presticides/PCBs analyzed by GC/EC methods. This flag identifies all compounds identified in an analysis at a secondary dilution factor. This flag indicates that a TIC is a suspected aldol-condensation product. Results are unusable due to a major violation of QC protocol. Cannot be confirmed by CLP protocols. DEFINITION Estimated or not reported due to interference. See laboratory narrative. Analysis by Method of Standard Additions. Spike recoveries outside QC protocols, which indicates a possible matrix problem. Data may be baised high or low. See spike results and laboratory narrative. --_, -- INTERPRET A TI ON Compound value may be semi- quantitative. There should be another analysis with a D qualifier, which is to be used. Alerts data user to change in the CRDL. quantitative. a possible Data is Alerts data user of a laboratory artifact in the TICs only. Compound value is not usable. Compound may or may not be present. INTERPRETATION Analyte or element was not detected, or value may be semiquantitative. Value is quantitative. Value may be quantitative or semi- quantitative. l!!!!!I ------ * * + + [ ) B UJ J u u M II R llaste Cbatactei:istics A -Toxic D B -Corrosive E C -Radioactive F - - -- Duplicate value outside QC protocols which indicates a possible matrix problem. Correlation coefficient for standard additions is less than 0.995. See review and laboratory narrative. Value is real, but is above instrument DL and below CRDL. DL is estimated because of a QC protocol. DL is possibly above or below CRDL. Value is above CRDL and is an estimated value because of a QC protocol. Compound was analyzed for but not detected. Duplicate injection precision not met. Post-digestion spike for furnace AA analysis is out of control limits (35-115%), while sample absorbance is <50% of spike absorbance. Results are unusable due to a major violation of QC protocols. Identificaticc* -Persistent G -Flammable -Soluble H -Ignitable -Infectious I -Highly Volatile -I!!!! I!!!!! 11!!!1 J K L Value may be quantitative or semi- quantitative. Data value may_ be biased. Value may be quantitative or semi- quantitative. Compound or element was not detected. Value may be semiquantitative. Compound was not detected at or above the CRDL. Value may be semiquantitative. Value may be semiquantitative. Analyte value is not usable. -Explosive -Reactive -Incompatible Giiiiiiil I .. I I I I I n I • D D n E m E I ' I APPENDIXB SITE INSPECTI10N FORJ.\1 POTENTIAL HAZARDOUS WASTE SITE I. IDENTIFIC..l TION --,SEPA 01 STAT'E I 02 Sil'E "IU""8ER SITE INSPECTION REPORT NC I D000813592 PART 1 • SITE LOCATION AND INSPECTIOM INFORMATION' D II. SITE NAME ANO LOCATION 01 SITE NAME lt•a., ,......._ "'~'''""'',..•"-•'""•' 02 STREET. Aoure NO ~A SPECIFIC LOCATION IOE/'ITIFlEA Georgia Pacific Corp. Hardwood Sawmill Plywood Drive CJ ClfY o•sure \ 0!I ZIP COO~ Cl! COUNTY ,:1cou7 oe CONO I Washin°ton i :coe ~ST D Plymouth NC I 27962 1094 01 09 COOROIN.,iES I \ 0 NPE OF QWNEl'lSHIP IC•or• ..,,., U.TITUOE \ :.ONGITUOE ~A.PRIVATE O 8. FEDERAL = C. STATE Q 0. COUNTY : S. ",l:UNICIPAL :150 SJ..'.. J. Q'.' . I _]£ o ..41.c .JQ.'.'. CF. OTHER ~ G.UNKNOWN D lll. INSPECTION INFORMATION 0 1 DA TE CF INSPECTION I o,s,TE ST .rus OJ YEARS OF OPERATION z , I I· 21 :X ACTIVE 1950 I I983 _UNKNOWN "°"'"" a•, •f •• C iNACTIVE 3EGt,,jNl"IQ YE4A :NOINC, YfAR I 04 AGENCY PEAFQFIMINGlkSPECTIQN ,c,..,., .. ,,..,_, ~ A., EPA C: 8 E?• CONT~ACTQR ~ C. MUNICIPR C: :J. MUNICIPAL CONTRACTOR Greenh·or·ne~'o I Mara ~--,_ ':: E.STATE ~F S7ATECO~TRACTOR '= G. OTHER .. _.,,_, ·s,i.c.-,1 I a~ c,.a1EF IN:;PECTCA l 06 TITLE 0 7 OFIGANllA TION I~· :~~';;:088 .Jeff Tvbnrski r.,:)0 1 ......... ist nc_n ::>9 QH-sE" ,NSPECTOAS 110TITLE ; I OFIGANllA TION ·: ~ELEPI-IONE ft,fQ I I Jerry Johnson Land Surveyor G&O , i9191 782-9088 l I Christopher Huff Environmental Engineer G&O I ~191182-9088 I I Grover Nicholson Environmental Engineer NCDEHNR 119191 733-2801 I Harvey Allen Environmental Engineer NCDEHNR I 919 1733-2301 -· I I I I : J SI re AEPAESENTA rives INTE'=IVIEWEO \~TITLE 1 ~AOOAt:SS \ '. e rEL£PMONE NO nvironmental Jav Johnson Manager Outer Banks Contractors I ' ' I I I ! j I I I I I I ! I I I I I I 1 1 ACCESS GAJNEO 8Y I,, nM: :, 4 :s,ecm" 19 WE,.THER CCNOITIQNS ·C~u• ..,., ~ PERMISSION Overcast, cloudy, chance of rain 80-85° I 0 WARRANT IV. INFORMATION A\/AJLABLE FROM 01 CONU.CT 02 OF ,..,v•,..,.,°'9_._,, OJ TEU.PHONE MO. I Grover Nicholson NCDEHNR-Superfund Branch 19191 733-2801 o, PERSON RESPONSIBLE FOR sire INSPECTION FOAM 05 AOE~Y oe OFIGANIZA TICIN 07 TELEPHONE NO. oe OATE IQ· 131 191 Irene Mendoza G&O (301)982-2800 -:,N"OI Q,lY llE"" '€PAFQRl'2070-'317 On I D -,EPA HA ' SITE INSPECTION REPORT, : t ST.1.f'E 102 S1;: '<U.,.8ER NC I D000813592 PART 2 · WASTE INFORMATION POTENTIAL I IOENTIFICA TlON ' 'I. STE ST A TES. QUANTITIES. A.NO CHARACTERISTICS PHYSICAL STATES ,c,.,.u .. ,,.,.,_,, ' J2 WASTE QUANTITY Al SITE OJ W,1,,SJE CHAFIAC1E::Isr~s ,c.,,u ~,,.., -· l ,., .. .,, .. "' ,.,.,. ow•.,M••• X • raxic .~ ~ SOLUBLE _: i Hl(JML • ·•CLA rlLE ~ SOL :0 E SL:.;RRY < -wJt .:>• -"O~.-,.-a,,.tt 3 PQW'.:lE~ H•;ES XF L'OUIO ' '.:)NS lJL.3~ =I..:-; r _ a CORRC)SI~ E : ~ 1NFECT10US _: ; f).PLCS.'YE _ c R•o•o.,c::·,e _: ~ FLAl•ll•'-'8LE : ,,; Re•c-,·,e X: 3LUOGE G GAS x:i PERS1:;;~..,T :. "' •GNITABLE : ~ INCQ._.P,T!BLE : ."'J•S Y .t.FIOS -· . --------·-: '-4 N07 .;.,'PL1CA8LE ;: ... f.-l -------~ :~,-,,., •,Q QF :)RUM~ .. -------- : Ill. WASTE TYPE -~::O"' I SUBSTANCE .•u.ME j O, GROSS AMOUNT 02 UNIT QJ: Mf,t,SURi: I CJ COMMENTS SLUDGE I 1/; ""' nounds (KOO 11 waC"+-ewater sl·"~e OLY'I OILY WASTE I 20 000 nounds i (DOOO D007 D00081 snent oil rl SOL SOLVENTS 375 oounds ( FOO 1 . Fons ff'lQi;\ --.1••-.,t-c .::,50 PESTICIDES U.,..l,-unknown lindane f..:----.... .:-..:,..:i,..) ')CC I OTHER ORGANIC CHEl.41CALS rfi OC I :NQRGANlC Cr.€.i..4•CAL5 .:.co : ~cios I I 3.:..5 3ASES ' I ,,,::_s ' --€AVY MET.a.LS ! I . HAZARDOUS suasr ANCES 1.s, ...... _. ,a,_,,,,u .. -,,.. , ..• :LAS N-=••11 I -,:,_rEGQAY j ·?2 SUSST ANCE NAME I OJ CAS M,JMBfR :i, STQR,t,GE1oi':,i:ics.1.L ME TMOO ! C5 CO-~CENTA,HIQ\, I ~a MEASURE OF CONCENTFU.TIOH ii Chromium I 741,n 4 7 -1 drums unk----- ! Lead I 7439 92 1 drums unknown I ES Pentachloronheneate I 87 86 5 drums unknown IC I Sodium Metaborate drums I unknown I Chloronhenols drums unknown I Lindane i 58-89 9 drums i unknown I ' I I I I I I ! I I I I I I I I I I ' i I I I I I i ' Iv FEE0STOCKS ,s .... .,..,,..,_c .. s- CATEGORY I 0 I Jll:E0$TOCK NAMf 02 CAS NUMBER CA!EGOAY I 0 I FEEDSTOCK NAME 02 CAS NUWBEA =os ' FOS I ! I =-.:s I 'OS I I =os I FQS I .:os I I '0S , lv1. SOURCES OF INFORMATION ,c •• ,.,"'~" ,.,., ... c ... • o ' ·'" , ... ·-·· ....... ,,. , ......... , . 1. G&O Field Notes I 2. NCDEHNR-State Files 3. Sax & Lewis; Dangerous ProEerties of Industrial )!ate rials -tt """ ,. ,. "" " I n R n I I I It I I I I \ I I .r1 I , I I I i I I I \ : i ' ! ! COTENTIAL HAZARDOUS WASTE SITE SITE INSPECTION REPORT i :. 1DENTIF1CAT10N NC D000813592 ,SEPA Pj\RT J • DESCRIPflON OF HAZARDOUS CONDITIIONS AND INCIDENTS IQ\ su.re 02 SITE NUMBER ·1 1-4AZAR00US CONDITIONS ANO INCIDENTS .. .. ' u;:;ouNOWA TEA CONTAMINATION 02 C OBSERVED !DATE _ POTENTIAL ·~ ALLEGED -9,863 : J c,:c•~·•~:. '."1C,",' POTE"<TIALL Y AFFECTED -.::.; NAARATlVE DESCRIPTION Groundwater wells located within a 4-mile radius of the site serve an estimated 9,863. : 1 ·...: = SURF ACE WATER CONTAMINATION 02 G OBSERVED (DA TE: = POTENTlAL :J ALLEGED :2 OQPULAT!CNPOTENTIALLY AF;:'fC':"i::D Jd NAAAA rive OESCAIPTtQN . There are no surface water intakes within F ·' miles downstream of the site. .. :2NTAMINATIQN QF AIR 02 C CSSEAVEOtOATI: . ) :: POTENTIAL ~ ALLEGED :-: -·= 8,172 : J 0':l='L:L.:... T\CN POTENTlALL Y At=;:-:_,: TED ~4 NARRATIVE DESCRIPTION There are an estimated 8,172 residents living within a 4-mile radius of the site. :: . ;e:;:iE.'EXPLOSIVE CONDITIONS •:::2 C! CBSERVEO (DA TE = ?QTENTIAL 0 ALLEGED --:J P,:,01_1t.ATION POTENTIALLY AF;:~CTED ------.}4 NA.AAA TIVE DESCRIPTION After a fire in 1983, The Georgia-Pacific plant was permanently closes and ooerati.nn~ r:cased. o, =-: t=: JIRECT CONTACT 02 :_:: CSSEAVEO !OAT,E : C POTENTIAL 0 AU.EGEO :J POPULA TlQN POTENTIALLY AF;:ECTEO 0-4 NA.ARA nve OESCF.IPTION N/A _, -co.-.,4.MINAT\QN OF SOil J2 :: CSSEAVEO IOATE ' ,_: POTENTIAL :J ALLEGED :,J .:.;;;EA PO":'E!'ITIALLY AFFECTEC ·24 NARRATIVE OESCFIIPTION '('OIJ Chlo roe thane was detected in soil sampling in the vicinity if an alleged TCE ,· •mill . Also, pesticides and:metals wre detected in soil samples take rt dliringi:the I site visit. ~ J\ ,_ G CRIN!';INGWATERCONTAMINATIQN 02 0 OBSERVED (OAlE. : ·-POTENTIAL ·...J ALLEGED OJ POPULATION POTENTIALLY AFFECTED 9,863 0-4 NA.ARA TIVE oesc1='.1PTlON Groundwater wells· located·:within a·.4-mile radius of the site serve an estimated 9,863 residents. •J\ ._ ~ WORKER EXPOSURE/INJURY 02 0 OSSEAVEO (□Are. I '.J POTENTIAL 0 ALLEGED ' -JJ wQAKERS POTENTIALLY AFFECTED Q,4 NARA A nve DESCfllPTION The site is unoccupied and inactive. -: '. __ , ;iQPULATIQN EXPOSURE/INJURY 02 0 OBSERVED (DA 1 E · I 0 POTENTIAL C ALLEGED OJ PCPULA TION POTENTIALLY AFFECTED. 04 NARRATIVE OESCHIPTION N/A H POTENTIAL HAZARDOUS WASTE SITE SITE INSPECTION REPORT I. IOENTIFICA TlON PART 3 · DESCRIPTION OF HAZARDOUS CONDITIONS ;IND INCIDENTS AZ.AROOUS CONOITlONS ANO INCIDENTS ,c~ .. ,.-.. n• ,)2 G OBSERVED IOATE ___ · ____ , : POTENTl.&.l Stressed vegetation was noted in the area of the alleged TCE spill . N/A l_ ,11 : •-c.:::~;iJ..i.AINA.nON oF FOOD CHAIN :1I"4 ,-.;AP~A; • :;. -::::SCRIPTIQN i N/A l _ •.1 .";$".l8LECONTAINMENTQFW&STES 02 C ::BSEAVEO !DATE ------' 02C:OBSEAVED!OATE '. : POTENTIAL ·__: ?OTE~TIAL :,4 N,11.PAA TIVE DESCRIPnQN = ALLEGED .:; ALLEGED :: "-LU:.G.EO I Lumber was passed through a dip vat on a conveyor system. was allowed to drip drv onto the ground. The wet wood 01 _. :,:.v.:.GE TO QFFSITE PFIQPERTY )2 ---~ CBSERVEO !DA TE ----~-' : A.LLEGEO ,1:, '"'""'''' :;sca,PnoN N/A • POTENTIAL .• ALLEGED N/A :-2:. OBSERVEO!OATE --------' POTENTIAL : A.LL.EG.:O 1)5 cc.sc;;1pt,,:-. OF ANY OTHER KNOWN. POTENTIAL. OR ALLEGED HAZARDS N/A , I. TOTAL ;:iQPULATION POTENTIALLY Al'FECTEO: ~.172 <4·milel IV. COMME~TS SOUACES :;F INFORMATION,c~ .. , ..... , ........ ..., ... J .,.,., •• , ,.._.,..,.,,, •• ,_,.. 1. G&O Field Notes 3. USGS Qua,drangle Maps I ' 2. NCDEHNR Files -------. ---------------------------' I ! POTENTIAL HAZARDOUS WASTE SITE I 1. iOENTIFICA T!ON I ,&EPA SITE INSPECTION \o:~~ue: :h~~~u;~~ ~ ~'> ---?ART 4 · PERMIT AND DESCRIPTIVE INFORMATION AMIT INFORMATION a -. =!: OF" ;,':.:i,..1r 1$SiJEO :;;: PERMIT NUMBER , :J DME ,SSt:EO IO• ElPIR.lT!ONO,UE \ O~CQM1t,,1fNTS : -., '.,,. ,.,. ,ooo .. I I ' '-IPOES i ; -- -IJ\C I I I I -AIR i I - ;;:cA.t. ; I I -' --ACRA INTERIM ST A TUS 1 NCD0008 I 1'iG2 I ll il?/0/1 I I -, SPCC PLAN I I I j ST A TE ,sa,c,,., I I --LOCAL • I '~"f"•' I -. )THEA ,s0..,,.., I -.;QNE i Ill. SITE DESCRIPTION I -: ·-~q-"GE,c,sPOS"L -~ •• ,. ,< '"'' •oo .. , =~ .1.J.IQUNT ·)3 UNIT OF" '-'E"-SUAE 1 -:, <AEATMENTrC11n,.,.,,..,_, I °' ors,, _: ;. SURF.6.CE IMPOUNQMENT = A. INCENEF.A TION -P•L:S : 9. UNDERGROUND INJECTION . :{ 1 e..:;:.:1NGS ON srre -Xe JFl.UMS. A.8Q'JE GROUND 10 C tonsLy_r. : :::. CHEMIC.,UPHVSICAL i I --TANK A.6Q'✓E GROUND = .J. BIOLOGI :AL I ---TAN)(_ 8E~ :·.-.. GAQUNO : ~-WASTE OIL PROCESSING i JIS AAE• c: SHE - -C _:..NQFllL i :_ F. SOLVENT RECOVERY I '3 LrNOFARM i : G. OTHER f!ECYCLINGIRECOVERY 25 i•ctNI I : .; OPE;.'-./ DUMP -" OT~ER I I -. !..o.u"Y1 _: 1. OTHEFl i ::.,_., O" ::'-o.lENTS ' I IV CCNTAINMENT I -.: .:r.-:-.I.INM€.NT OF N•STES ::.•oc• -•• = I.. .\DEOUA re. SS.C'JAE = 9. MOOERA re ZJ C. :~ADEQUATE. POOR ~ D. INSECURE.UNSOU~O.CANGEROUS C< ; :SCRIPT1QN OF OPU,_.S :;:1K1NG. LINERS. 8-'AAlfRS. ETC. I Lumber was passed through a dip vat on a conveyor system. The wet wood was allowed to drip onto the ground. Also, it was noted during a 1981 site inspection that a tank used in the wood treatment process was found to be leaking. I . V ACCESSIBILITY : 1 WASTE E,i,SILY •CCESSIBLE: CJ YES = NO I : : ::::,..1.1E'°<TS Details regarding the accessibility to the drums during the years of operation is not known. Access to the site is limited by fencing and a gate guardhouse. VI SOURCES OF INFORMA. TION 1c,, 10.•""" ,.,., ... c.,_, o ,,.,. , • ., ,_,.,,. .. ,.,,, ,,.,..,.u 1. G&O Notes 2. NCDEHNR Files I I 0 I. IOENTIFICA T!ON n POTENTIAL HAZARDOUS WASTE .,ITE SITE INSPECTION REPORT 02 SITE OjUt.18ER ?ART 5 ·WATER.DEMOGRAPHIC. AND ENVIRD~IMENTAL DATA D000813592 KING WATER SUPPLY 'IPE OF :;:lRINKING SUPPLY •.c•u•O-•-• SUAF&CE ·]2 STATUS :J 01ST ANCE TO SITE WELL :.~OANGEAED -'\F~ecri::· •~ONITORED :.:::MMUNlrY A. 0 S. j! ' C B C. 0 ' 1. 2 'ml) -COMMUNIT'Y C ,-. J l! J C: E -~ 3 (mil - ROUNOWATER GROUNQWA, TER USE IN VICINITY 1C•oc• ,,..., r .:. CNL V SOURCE FQR ORINl(ING : 9 0RINl<ING c,~., '""'"' •~•-• co,.o,1eRCU,L. INOUS~RIAL. IFIMJGA TION ... o .. ,.., •• ,., ,_ ..... ._, ~ C CCMMERCIAL. INOUSTR! ... l. lRRIGATIQN = :,, NOT USED. UNUSEABl.E ,V-..... ,,., , .............. -1 :ll0Puvr,,:NSEF1veoevaRouNow1.re11. 9,863 (4-miles) 03 DISTANCE TO NEAREST OR INKING WA TEA WELL 2.7 (mtl 3.5 j C~ DIRECTION OF GROUNOWA TER FLOW northeast 08 OEPTM TO .>,QUIFEi~ I 07 POTENTIAL YIELD OF CONCERN OF AQUIFER 150 " :0001 08 SOlf SOURCE AQUIFER =iESCRIP ;,.:-~ OF WELLS ,,~c,.,.,.,.o ~•ut• :oo,,. ,,.., -•,_, ,., • .,._ ,._.,..,_, -o.,..._11 I The City of Plymouth Public Works Water system uses 4 wells having an average depth of approximately 175 feet; 3 of the wells are located inside the city limit and the 4th is located within 1 mile of the city limits. Private wells within th studv area are enerall 200 feet deep . • EC:-. ... .:lGE •AEA I (ES COMMENrs .= YES Cl NO I CCMMENTS __ NC I FACE "'•TEAUSErC~•:•o"•' A RESERVOIR. RECREATION DRINKING WATER SOUF\CE ·= B. IAAIGAT10N. ECONOMICALLY IMPORTANT RESOURCES = C. COMMEFICIAL. INDUSTRIAL = 0. NOT CURAENTL Y USED ,.F;ECTEO. ?OTENTIALL r AFFECTEO 800-ES OF WA TEA AFFECTED 01ST .A.NCE TO SITE 0 5.7 ---------------------------------------- DEMOGRAPHIC AND PROPERTY INFORMATION TQT AL POPUL.4 TION WITHIN 0NE I 1) MILE OF SITE l'WO (21 MILES OF SITE , 2. 240 a 4 482 -.o o, p,~q5,()f,o!, -.o o,. i,111so,,rs THREE (31 MILES OF SITE C 6,573 ..0 OJ l>fllSO,.~ 02 OlST>.NCE TO NEAAEST POPULAIION _______ _,m,1 (mo ~J ~UMOEA OF BUILCINGS WITHIN TWO 121 Mll.iso, SITE O• 01ST ANCE TO NEi,REST OFF-SITE BUILDING ii I I 1,651 ;,O?ULA.!•0"' WITHIN VICINITY OF SITE ,_...,_ ....... .,.. • ., • .c, _ _,,..,..,. 0 ,_.,..,_, .,.,..,._..,.00,,_0 •: The nearest residence is located approximately 700 feet east of the facility Plymouth High School is located on the property approximately 700 south of the facility. A baseball park and a residential area are located adjacent to the facility to the south. H POTENTIAL HAZARDOUS WJISTE SITE SITE INSPECTION REPORT ~EPA PART 5 ·WATER.DEMOGRAPHIC. ANO ENVIRONMENTAL DATA · i\. ENVIRONMENTAL INFORMATION I I IDENTIFICATION lo, su.re102 SITE NU1t.18ER NC D000813592 :o-• -1 c-J cm,,..c ,_: : GAEA re.:;, THAN IQ. l cm1sec --: 5 RELATIVELY IMPERMEABLE :o·• -•o·~:-uc, X C REU TIVELY :JECIMEABLE ,,-; • •o·•:.,,.c, '✓ERV PEFU,AEABLE ,=., .. ,.,,,..,. ,o·l•~•o-c• O• DEPTH OF cci-.r U~!NATED SOIL <.ONE ml -------•,Ill oe SLOPE I j :o NET PAECIPIT A TIQN I 9 I :a ,,oc: >OTENT>'c :in) SITE SLOPE I CIRECT!ON OF SITE SLOPE I TERRAIN AVERAGE S~OPE ~~2~---" Northeast 2 " ~ SITE IS ON 8ARAJEA ISLAND. CC·ASTAL HIGH HAl.l.A0 AREA. RIVERINE FLOO0WAY I' 51 TE iS •N • ~ ,R FLQOOPL.A.IN ', J157Al'<Cf TC-1>1ETLANOSrl1c,•-• i I 2 01ST A"'CE T•J CRITICAL r,ABITA T 1~ --,.•• ..,.c•u I I I I 11 ! =:STUARINE ! _____ [mil (m11 a. I ENQ.A,,.,,GEAEO SPECIES. JISTANCE TO ·:::JMMERCIAUIN0USTRIAL ::i: S!QENTIAL ARE .a.S. NA flQN.a.L'S7 .,_ TE PMH<S. AG RIC UL TUR.4.L LANDS FORESTS. OR WILDLIFE RESERVES ;,ci+ME AG LANO .a.G LANO B _0"-'-.-=-lcc.3 __ ,m,1 C. _____ [m1J 0. ______ {m1) 4 oe SCR1PTIQN OF SITE IN REL.a. TION TO SURROUNOJNG roi:,OGR.a.P ...... The Georgia Pacific Hardwood Sawmill site is on a relatively flat parcel of land surrounded by the Roanoke River on the nothwest and wetlands around the remainde of the property. It is located in a region characterized by extensive, flat coastal swamps adn marshes. Elevations in the vicinity of the site are slightly above 5 feet NGVD aro;und the facility and slightly below 5 feet NGVD in the nearby wetland area. '✓ 11. SOURCES OF INFORMATION ,c.,. ,.,~,.c,,,., • ..., .. • 0 . .,.,.,,., .. _,. ... _, .. _ ,_u 1. NCDEHNR State Files 5. So:Ll Survey for Washington County 2. USGS Topographic Maps 6. Groundwater Bulletin for Swanquarter 3. Rainfall Frequency Atlas 7. G&O Field Notes 4. Cliamtic Atlas of the U.S. B POTENTIAL HAZARDOUS WASTE SITE I. IOENT1F1CA TION l~E:~N 01 STAf'E\02 S{TE NUMBER SITE INSPECTION REPORT NC D000813592 PART 6 · SAMPLE AND FIELD INFORMATION I \o' ~uMBEA ~ c: S,O.APLES SENT ro ClJ ESTIMA Tl:0 OA TE s~...,.PLE T'(PE SAMPLES T _.,KEN R:E.SULTSA\/AA....a..f : c;.::iQUNOWATER I 1 I ... rl.1~t-ri .,:il .-..,,.:i 'C'.-.H-: e...,..,..., 1 II 1 .. er ( T ro • ~ ' I SL..'~F•CE WATER ! / 2 State Analvtical Laboratorv (SAL) ' -! "NA STE ' i ' I I >,R I I ; C I rlUNOFF I L I SPILL I ' r SOIL I 2 I IEA ii .,GE7AT,QN I I ' I I I ! :_:-,-e;::i. ! 2 SAL I FIELD ME.SUAEMENTS TAKEN r,-i:>f 02 CQMMEf'(TS I pH Temeerature Conductivitz I GW6W01 'i 'i lQ? or. 1 0 A-n Al GW6W02 18.4-27.0 0.27 i i I Jv PHOTOGRAPHS ANO MAPS . -. =-€ X UROU:".Q X ~ERI.A.L l C2 :~ CUSTODY Cl'" GI:~~llbQi;:ne & Q' Mar~ 1 Inc. ... -... _~•q.,..,,.,_.,__, C.'.l M.l.::>S ; : ~ 1..oc,i.r1ON OF M•Ps I X ,·es Gi::eeDbo:cne & Q'Mara. and NC!lEHN!l SllperEund B:cancb ·.o I V. OTHER FIELD DAT A COLLECTED ,,,.,_ ............. ,c,.,,_, I I I I I I Vi. SOURCES OF INFORMATION :c,,. ,0 K.,,. ·•••••ncu • g ,·,·•••fl ,.....,..,•n•'-••• ,op,ollll 1. G&O Field Notes ~ 2. NCDEHNR State Files AFQFH,,,1 "2070•13 t1 1!11\ ff POTENTIAL HAZARDOUS WASTE SITE ;1. IOENTIF!CA TlON .n EPA -SITE INSPECTION REPORT lo\ ST ATE \02 SITE -"'UM8Hl PART 7 • OWNER INFORMATION \ NC , DOOOR[>Sa7 111. RENT OWN ERIS) I PARENT COMPANY,,,,_._, • .... Ee 1.;2 o .. e Nu...-eeA 1011 N,Oolf \09D•S-.uwafA I I (11,rer n.,,.,,,J~ .... rn,..,-..,..,,.,,.,,.. ......... ~ I I !:)STPEET •UDflES.S ' : 3o, ~,;;, ,,c ' 1o•s1ccooe \: 0 STl';EET •ODAESSj,, o ll<u iUDI •«, I S.C CODE :I=-I ' 1-:~Sl.&.rei::• ~:PCCOE i : ~ CITY ·JSTATfj1•l:PCCCE ' i Plvmouth I NC I I I j ....... ,t; 1.;2o•BNUMBEA \ 011 NAME \°90+81'1UM8fA I I I r'.lJSfl:tfET•OOAESS ~0 &., ~•O• ,,c, 10• sic cooe l,o stAEET ADDRESS 1, o a..,. IVO •. ••c I r' SIC :□DE f c,r, r!ISTATElo; ZIPCOOE ! 12C1T'I' \1JSU.TE 1 • liP CCOE I :, I "'"' ... E j 02 :1+8NVM8fA l OIi NAME 09 0+8 '"1.IMBEA sr=~~T •ODAESS ''=' a.o, ~,o, .,, 1ci• SIC CODE l tO STREET AOOAESS'1 .. 0 .... A~o,.,,c1 i , ~ CODE l I ,c,,, I r6 STA TEI 01 ZIP COOE ! I 2 CITY I 1J STATE\1• l1?CCOE . I I I I.JI ...... ,.,t, \C2 D+QNU~BEA 08 NAME \090•6-.IJMSEA J,, s; "" ,ooses, •? 801 MO• ,ic, 10• SIC CODE ,o STREET AOORESS1P O &o, -.10, .,,.1 r~$.ICCOOE ti'" r· ST" or llPCOOE 12 CITY I\ J STATE '4 l,P COOE PREVIOUS OWNERIS\·~·••~11••c-••••1 IV. REALTY OWNEA(S) 1~•--· "''"°"'..:, ... ,~.,, Ql NU,11; 02 0+8NUM8ER 01 N•Mf 02 0•8 '°IUM8ER I n,..,ratur Par ...... erc::hin JJ S7?fET AQQAES.S • o ~o• ~,,, ••<, ! oc sic cooe OJSTRffT.lr.OCAES!;rPO ao •. ,vo, ., .. , ! :, SJCCODE i I o:. c1:, \ 08S:;E( ,:,; ,:1P CODE 0!.i CITY \ oe ST.Ir. TE\ 01 l:P CODE J..T...,,...,...she...,,.:i 01 ,....,..ii; \°20~8NUM8ER 01 N.1,Mf j :::;•il-.uM8fR I ~,,,_,...,.,.,...i:::r _p,.,,...;Fir r, --......... OJ STREET .1,,QORES.S "o 11o, ;i,o, ••• ! 10• SIC CQCE OJSTRfET.i,,OQAE~,PO ao,.1110,.,,c.1 I:• SIC CODE Pl ..l n-.: .. O!.IC1;"",· 1::TATE 07 ZlPCOOE 0~ CITY loesure 07llf'COOE I Pl ·--rh 27%2 01 NA.Mf 02 0♦8NUMBEA 01 NAAtE 020•8NUM8fA Atlas Plvwood I OJS:;iff~AQ()AES3 °,; s.,, ~•.;. ••<• 10• SIC CODE OJ STPl_:E! AOQRESS,P O ao, .. ,o,. ••< l i J• SIC CODE Plvwood Drive ! O~CtTY 1:::TATEI 07 ZIPCOOE O~CHY l°6ST,t.TEI01 ;:PCOOE I Pl um,..,, .,.}.,, ?701'.? ·,1_ SOURCES OF INFORMATION ,cuoo_,.,.,._ ... , . ..... , ... _,_ ... ___ ,_., I I. NCDEHNR State Files P.&.FQR"42070-IJ;; 1111 I n POTENTIAL HAZARDOUS WAST,E SITE SITE INSPECTION REPORT PART 8 · pPERATOR INFORMAr'ION L IOENTIFICA TION QI SU.TE 02Sl~ENUt.lBE.R NC D ? UARENT OPERATOR ..• ...,..., •• _.,_,_., .... ,, OPERATOR'S ,='A,qENT COMPANY ,~•-•-• Banks Contractors, Inc. 1020+8NU"'48EA O• SICCOOE Q6STAfE 07Z1PCODE I :p1 mouth NC TE,vlSQFOPEt:l•TION 09NAMl:0F0WNl:A ia Pac·f·c ! )J sr:=.!:CT •OORESS ,,.0 ao, ,.,o, 1 wood Drive !Plymouth a 02 0 + 8 NUMBER O• SIC CODE 06 sr.ue, 07 ZIP CODE NC 02 0+8 NUMBER 04 SIC CODE 05STATE 07ZIPCOOE 02 0• B NUM8EA 04 S•C COOE OC!STATE 07 l!PCOOE 8 YE.-"JI.S OF OPEAATIQN 09 NAME OF OWNER OURING THIS PEA,00 I I 0+8NUJ,,1.8f,R 2 STREIT AQQFIE!~ ~ o So• 11,0, ore, \1J SICCOCE • CITY PREVIOUS OPE:R.UORS' PARENT COMPANIES o,..,_,.,., ·ONAME 11 O+BNUholBEA :2STAEETAOOAE~S •o 1o,.11,o, flCJ I' J SIC CODE ; • CITY 1•~STATE ,ez1PCOOE I 'ONA.ME I' 1 o ... eNu...,,seA • l STREET ,1iQQAES:> .• o So, . .oo ,_ 1,c 1 1 J SIC CODE : • CITY l~STATE l6Z:IPCOOE 11 O+B NU""'9EA 1J S1CC.OOE '. 4 CITY 1!lSTATE 1ez1PCOOE IV. SOU ACES OF INFORMATION ,co __ ,_,.,_n •. , .. .,.,.,""· •--••" .,_., 1. NCDEHNR State Files _I I I PA OFF-SITE GENERA TOR(S\ Tl.EE T •OOAESS ,., o &o•. AIO • o,c, J 5:PECT .t.QOFIESS ,P 0 801 . .-,o, ••c, 5 CIN POTENTIAL HAZARDOUS WASTE SITE SITE INSPECTION REPORT PART 9 · GENERATOR/TRANSPORTER INF'ORMA TION ! Q• SIC CODE 01 NAWE IO• 5'C CODE OJ STREET _.,OORES~i ,,. o ao,. 111•; • "c, r6ST.4.TE 07 llPCOOE 05 crrv 1cc STATE 01 llPCOOE I I 1020+8NUM8EA 015 Sf.I.TE 01 ZIP CODE -:, SICCOOE OOSTATE OIZIPCOOE !JI NAME OJ STREET AOOAESi 11> o i,o, ~ 01 NAME OJ STREET AOORl:S:; 1• o lo, ... ,; • "(./ O5CITV 01 N.6.ME 0JSTl=IEETA00RES5,,.o ao, .;,.,:;, ..c1 SOURCES OF INFC:1.MATION rcu a..c-,., .. ....,., •, "''"' .. '· •--.... ••-111 I. NCDEHNR State Files A~0RM2010-1JO·&ll ! 1. IOENTlFICATION I::: 1 STA TE( 02 SITE NUMBER NC 1D000813592 02 0 + 8 NU1rrio18ER o• SICCOOE CG STATE 01 ZlPCOOE 02 0•8 "'U¥8ER IO• SICCOOE ;;155TA.TE 01 llPCOOE O20,..8NUM8EA o• SIC CODE oeSTATE 07ZIPCODE 02 0+8 NUMBER 04 SIC CODE oeSTATE 01 ZIPCOOE I RESPONSE ACTIVITIES : l ,, ~ TE.A SUPPL V CLOSED : ! ::Esc::::i':"'JQN N/A POTENTIAL HAZARDOUS WASTE SITE SITE INSPECTION REPORT PART 10. PAST RESPONSE ACTIVll'IES ' 02 DATE _____ _ M : ' ;E~;,,·:,~RARY WATER SUPPLY pcov,oeo N/A ·J2 CATE _______ _ I I I : : S;iiLLE0 MATERIAL REMOVED : .:. .:iesc.=,:?noN N/A -: : -:~NTAP,,m•./A TEO SOIL REMOVED : .:. oesc.c;;,,,-:-;-\JN ' N A : :: ,' . .:.5;e :::i:;0 •CKAGEO : " JESc.::1n10N N A -_, ·, .:.sre DISPOSED ELSEWHERE : .:. :esc?.:-'noN N/A : r, 0'1 SITE BURIAL : .:. DESCH:?TION N/A : I ., sm.J C~EM!CAL TREATMENT .:. JESC~ ::i71QN N/A : .i . .., SITU 81()L0GICAL TREATMENT : ! Jesc:=.1::i-:-10N N/A :•, SIT'..: ?"""SICAL TREATMENT : .:. oesc~;PTIQN N/A :: :. :,,cAPSULAIION -~.:. OESCFIPTIQN N/A = 1-4 ;:!..1EAGENCY WA::iTE TAEA™ENT : .:. DESCRIPTION N A :'. ,'-I C..:70FF WALLS -::.:. 0Escn1?nON N A :.•.•.!:FIGENCY 01KING1SURFACE WATER OtVEASIQN :.:. ;;esc:1_,:rnoN --:: :•.;:OFF TPENCHES,SUMP : ~ oesc;:.:?r10N 020ATE _______ _ U2 DATE ______ _ 02 DATE _______ _ ,J2 DATE _______ _ 020ATE _______ _ 020ATE _______ _ 02 CATE------~- 020ATE -----~ 020ATE _____ _ 020ATE _____ _ 020ATE _____ _ 020ATE ___ _ 020ATE ______ _ 02 DATE _______ _ I I, IOENTlFlCA TION JJ AGENCY )J AGENCY OJ .'IGENCY OJ AGENCY JJ AGENCY -JJ AGENCY 03 AGENCY 03 AGENCY OJ AGENCY 03 AGENCY 03 AGENCY OJ AGENCY OJ AGENCY OJ AGENCY OJ AGENCY OJ AGENCV g EPA P.&.ST RESPONSE .lCTJVITIES,c~•-i : : ::: A 8AAAIEA WALLS CCNST'RUCT'EO : -1 DESCRIPTION : : = S CAPPINGiCC'.'EA1NG : -1 DESCRIPTION POTENTIAL HAZARDOUS WASTE'SITE SITE INSPECTION REPORT PART 10 · PAST RESPONSE ACTIVlllES 02 DATE ______ _ ')2 DATE ______ _ -J2 DATE ______ _ I. IDENT!FiCA. TION C1 STA~ 015,1'E ~A NC D000813592 OJ AGENCY OJ AGENCY __________ _ OJ AGENCY __________ ~ I .;1 -X T BULi( iAM<AGE REPAIRED : -1 DESCRIPTION uring an Octobe~ 1981 site inspection, a tank used in the wood treatment process was I ' ·Jl Q U GAOUTCL:ATAINCONSTAUCTEO C4 DESCRIPTION 020ATE ______ _ )I:,; V BOTTOl.4 SEALED 02 Q,&,TE ______ _ :4 OESCRIPflON :::· ::.: -.V GAS C::;.•fTAOL 02QATE ______ _ : -1 OESCR1PTIQN ·: 1 .:_: ,:, FIA::; •:C~HAOL 02 DATE ____ _ -.:.,1 DESCRIPTION The plant burned partially and then closed in 1983. J 1 C Y LE>-CHATE 7AEATMENT 04 DESCRIPTION JI::_:. Z. AREA EVACUATED 04 DESCRIPTION .; 1 ~ l ACCESS TO 5;TE P!:5 TRICii:0 :)4 DESCRIPTION : \ = 2. ;:>C,PUL' TiQN AfaQCATED : ~ DESCRIPTION :)1 = J. OTHER ~EMEOlAL .i..cnvmes ,J4 DESCRIPTION J2 DATE ______ _ 020.A.TE ______ _ 020.A.TE ______ _ 02 CATE ______ _ 02 CATE ______ _ 111. SOURCES OF INFQRMA.TlON ,c ... u,K~c••••·•~••• •o. ,,.,,, .. ,. •-••~.,.,,. ,._., 1. NCDEHNR State Files OJ AGENCY __________ _ OJ AGENCY __________ _ OJ AGENCY __________ --' OJ AGENCY __________ _ OJ AGENCY __________ _ OJ AGENCY __________ _ OJ AGENCY __________ _ OJ AGENCY __________ _ OJ AGENCY __________ _ D;._ ___________________ --:--:---:---:---:--:-:-:---::::-::-::7----,'--!-;,'-.-!.:1mo~E;!'Njirij1FI,1c~•~r~1_00'-N"..,---_-_-_-_-_-_l POTENTIAL HAZARDOUS WASTE SITE r SITE INSPECTION REPOFIT !" 51'" 02 sme .svMBER PART 11 · ENFORCEMENT INFORMATION . ENFORCEMENT!NFORMATION I ~2 D!:SCA1PTION oF FEOEFtA.L. sure LOCAL .::l!:·:.uLA.TORv1ENFORCEME~ .1.cno,.. m I I ~ I i I I I I I I 1. NCDEHNR State Files A FOAM 2070-1317·811 , NC D000813952 • '-u D I I I I APPENDI:~ C I ANALYTICAL DATA It I I I I I I I , I D N.C. Dc_panrncnt of Enviroomcn~ SAMt'LE ANALYSIS REQ1UEST State uboratory of Public Health llcallh. & Natural Rcwurcc, Q /) P.O. Box 28047, 306 N. Wilmington Street Solid Waste Management D1vwon L£ I\ C.__.L/1 Raleigh, Nortb Carolina 27611 n -·te Number 9 4 )) 0 00 . 'l I 3 5 q '.?., Field Sample 1 Number / .!5 0 I D .. , A ..st1w ,ru... 1... L... J D NameofSite(gr,,-<;··)°'--· ac·,+;c:,,. -lJA({l)µ_)oud Site Location, PJ..Ua)DL(f"H'' k A,StfL,\_)g,-T[)N c..n. I b ) JID# 1 (o Date Collected 1 -9 -9 I Time /I: n 0 Collected By I I t3f , {E :.:.:, ... --- I Agency: Hazardous Waste Solid Waste __0upufund TCLP Compounds ---- I Sample Type : .. Inorganic Compounds Results(mg/1) Environmental Conaentrate Comments Arsenic = Bariu~ ~'t"L. t,~_~ \i ,,~ II I _ Ground water (1) Solid (5) T !?Tf 13 L.ftN K -vnr+ Cadmium - _ Liquid (6) Scl\A-E:-.oc.0Y \ Chromium :<.:•.··:,j ~;1..,& -_ Surface water (2) • Lead __ Sludge (7) ('.;,,,,..,..,._;o.. -p o,c.;,£ (. = Mercury :iUi'cHtllNn SH:) iDN I _ Soil (3) -Selenium '" - ./ Other (4) A14 IIAQU+l Silver Other (8) -- I --Organic Chemistry Inorganic Chemistry - I Parameter Resulu(mg/1) Parameter Resulu(mg/1) (rag/kg) Organic Compounds Results(mg/1) ..1L_P&T:GC/MS Arsenic benzene --Acid:B/N Ext. Barium carbon tetrachloride -----MTBE Cadmium chlordane --Chloride chlorobenzcne ---Chromium chloroform ----I -_Copper o-cresol Fluoride -m-cresol --= p-cresol -Iron - I -Lead cresol -- -_Manganese 1,4-dichlorobenzcne --__ Mercury 1,2-dichloroethane Nitrate -I, 1-dichlorocthylcne I --Selenium -2,4-dinitrotoluenc -= beptachlor Silver -Radiochemistry Sulfates bexachlorobenzcne I ---Zinc hexachlorobutadiene Parameter Resulu (PCl/1) _· _pH -hexachloroethane _ Gross Alpha _ Conductivity -methyl ethyl ketone -I Gross Beta TDS oitrobenzcnc ---pcntachlorophenol TOC -_ pyridine - I Microbiology -tetrachlorocthylene -trichloroethylene Parameter Resulu (Col/100ml) -2,4,5-trichlorophenol -_2,4,6-trichlorophenol I --vinyl chloride ---endrin - ~/;J../919;lm , Dale Received Reported b~ £ )\J.P.' 0 lindane -methoxychlor toxaphene Dale Repo :;i-~1-C/ f -Dale Exlrnctcd 2,4-D -2,4,5-TP (Silvex) I yO~~p ~ Lab Number 9l 2G,~'5 -Dale Analyzed O I -DIIS 1 \I) I (Revised 2/91 ... , --.•. ~., , .. , -. 0 N.C. Depanmcnt ol Environm••~ SAMPLE ANALYSIS REQUEST State Labontory of P~blic Hcallh lleailh, & Natural Resources P.O. Box 28047, 306 N. Wilmington Street Solid Wai;tc Management Division (~ L f\ c_ L ft Raleigh, North Carolina 27611 n -· e Number CJ 'f J) DOQ 'B: I 3 ...59 ,3, Field Sample Nwnbcr ___ --'/_o.5"'--'O"---/_/ _____ _ .. +.-A R,2:!J D Ol:i . D Name of Site(,-e.o Ca ·, Q, -Pll,c I t'c -.IA-µ) mruSite Location p L \'.\ rn O I l t I, 1,., h.s b ·, n (\ IDt'--C O. :.::, ) ·. == ) ,J Collected By ./J A,:S v'E._\6 ALLE A J ID# 17 y Date Collecttod '7-/ I -q / Time /(). 4-.5 D Agency: Hazardous Waste Solid Waste ✓supe'rfund TCLP Compounds D Sample Type Environmental Concentrate. Comments _Groundwater (1) D _ Surface water (2) _ Solid (5) _ Liquid (6) i/0 ft/,3iy8j) P::.. 137/ I I ' o Lsoil (3) _ Other (4) _ Sludge (7) _______ ... if-t::.S::.tce_J""-q;o:=D,1,cf;..S _ Other (8) ---------· Organic Chemistry Inorganic Chemistry Parameter ~ P&T:GC/MS Resulu(mg/1) Parameter Resulu(mg/1) (1111g/kg) ....J<:'.'.'Acid:B/N Ext. ____ _ MTBE J:C'... "B /!J:i9() /, otwm L :D.srrc::ow=---- Radiochemistry Arsenic Bariwn Cadmium Chloride Chromium __ Copper Fluoride Iron Lead __ Manganese Mercury --Nitrate Selenium Silver Sulfates Zinc Parameter Resulu (PCl/1) pH _ Gross Alpha _____ _ Gross Beta Microbiology Results (Col/lOOml) __ Conductivity ----"--- TDS TOC Inorganic Compounds Results(mg/1) Arsenic , =Barium ~~~"\;t~U\c[:1 Cadmium" -' Chromium 1• .. •:: i Lead _· -Mercury SUP[P.fU~!D SECYiQll Seleruum · · Silver Organic Compounds bcnu:ne carbon tetrachloride chlordane chlorobenzcne chloroform o-acsol m-cresol --p-aesol --aesol 1,4-dichlorobenu:ne 1,2-dichloroetbane Resulls(mg/1) ------ ------ 1,1-dichloroethylene _____ _ 2,4-dinitrotoluene = heptachlor bexachlorobcnu:nc hexachlorobutadienc hexachloroethane ------ methyl ethyl ketone _____ _ nitrobenzcne --pentachlorophenol --pyridine tetracbloroethylene trichloroetbylene --2,4,5-trichlorophenol ---'---- --2,4,6-trichloropbenol _____ _ --vinyl chloride endrin lindane· methoxychlor toxaphene 2,4-D 2,4,5-TP (Silvex) D N.C. Dcpanment al Enviroamen~ SAMPLE ANALYSIS REQUEST State uboraiory al Public Health I lcalth. & Natural Resources P.O. Box 28047 . .306 N. Wilmington Slrcct Solid Waste Management Drvilion c:. C,_ ~ C-: L ft Rllcigh, North Carolina 27611 I o• C Number 9 'i J) ao O a I 3 ...s''} o\ Field Sample Number /._5' {) I ;2 .. -U-A~illOO..b DNamcofSitc{'-,-epc2:,·,o, -C(J,Ct;t;C -'B¼lmLLLSiteLocation PL\6,rnn,1,tl\ 1,.,1.sii', tl'.)iTir:,, (Io. ) . ) Collected By .J.J /1 I\ k'fg Al L f A) ID# ·7 Lf Date Collectc:d '7 -/I -q / Time / D ; .2 0 D Agency: Hazardous Waste Solid Waste ✓supcrfund TCLP Compounds -- I Sample Type Inorganic CompoundJ Rtsulls(mg/1) Environmental Concentrate Comments Arsenic I --Barium ,·. ,,._ •.· 'L~\'1',·'"~ ·, --• ~ \~ :• \ , [I . ;. . I_, I ✓ 1 _Groundwater(!) _ Solid (5) --,c E. -0 I Cadmium __ ... ""'. __ .., 1i ••••·1-·· --Chromium __ Surface water (2) Liquid (6) voe-l&ictft?c &/---' . ' Lead --I J Mercury SUiit;\y~;8 SEb:t:~;i IV Soil (3) --_ Sludge (7) PF ..57TG~C]y-..:::., Selenium --Silver _ 01her (4) _ Other (8) ----I ----Organic Chemistry Inorganic Chemistry -- I Paromeler Resulll(mll/1) Parameter Resulta(mll/l)(•mg/kg) Organic Compounds Ret!Jlll(mg/1) v P&T:GC/MS Arsenic benzene ----L Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane <✓ Ws#/!1:/)i.-S </'l1/0 -~-----Chloride chlorobenzcne ----I , Chromium chloroform I ----__ Copper o-cresol Eo~~·~ <~~o~ Fluoride --m-cresol --= p-cresol Iron J...;;, Ii <o;; -- I ~<f,QP/Jtn Lead cresol ----1,4--dichlorobenune <;;/,O f!I'"'--__ Manganese --~ <D,10~/!(>1 __ Mercury 1,2-dichloroethane I ~ <"·'" ,(¥111 Nitrate = 1,1-dichlorocthylene --Selenium 2,4--dinitrotoluene ----heptachlor Silver -- I Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene Parameter Rtsulll (PCl/1) ----hexachloroethane pH _ Gross Alpha __ Conductivity --methyl ethyl ketone I Gross Beta TDS --nitrobenzcne -----pentachlorophenol --TOC __ pyridine -- I Microbiology tetrachlorocthylene ----__ trichlorocthylene Parameter Ruulll (Col/lOOml) --2,4,5-trichlorophenol ---2,4,6-trichlorophenol I -__ vinyl chloride -endrin --lindane ,ate Received '1£~'fi!"' Reporled by --__ methoxychlor toxaphene 8 fl-~~, Dale Exlraclc~/-'/) f-/S'-~ s· ale Reported 2,4-D ' --2,4,5-TP (Silvcx) I ~.~~c,~~~~r,lfN~il .. r?:·;~. '~~ Number 912627 -- -- I N.C. Oepanment ol Environmea~ SAMPLE ANALYSIS REQUEST State ubontory o/1Publie Health • I lcahh, & Nalural Rcsourcca P.O. Box 280t7, 306 N. Wilming1on Stn:cl n Solid w .. ,. M1n1gcmcn1 Division c.~ ~ c_ LIT Raleigh, Nonh Carolina 27611 .. le Number 9 4 J) Q() 0 6' 13 -5''] 2, Field Sampl,: Number /.5 0 /. 5 D . . ) . *Af\)j,JDO~ . r 1 . NameofS,1e('..,.e.pc'2:,10. -{11c1:tiC ...SfJk)mr:LtS1teLoca1100 ~L\6,ff'CJl!t \ (Ah.sli1 tJfsillt:::-(1 I), 7 ) . D Collected By .JJ l'l ,S k'E.J:6 Al LE A ) ID# :7 y Date Collected 1 -I I -q / Time /,'§ ; 'f 5 Agency: Hazardous Waste Solid Waste VSuperfund TCLP Compounds ----' R Sample Type IDOl'l■ nlc Compouou Results(mg/1) Environmental Concentra1t Comments Arsenic Ll{,,":1 •9,1:,,,, -11 :, --Barium :-..,,,'t~ .._ .. _:., l, ; ____ .~_;/ B __ Ground water (1) Solid (5) LlJ tel {3[2 -Q l --Cadmium --Chromium '. ilOttLPiNtl.l ft!.&) --__ Surface water (2) Liauid (6) Lead ~u;j;:-,1.:-y"/i\ 0r-:: ' •: I -. I I I --I 11 11-0CO .. ;,,.,,~ I Mercury Soil (3) _ Sludge (7) J°[s rJ:C'.Tf>:"? --Selenium --Silver L 01her (4}St...DDn, ,v, Other (8) -- I ---- Organic Chemistry -- I Inorganic Chemistly -- Parameter Results(mg/1) Parameter Results(mg/l)i[mg/kg) Orpalc Compounds Results(mg/1) VP&T:GC/MS Arsenic benzene ✓ Acid:B/N Ext. ----Barium carbon tetrachloride MTBE ----Cadmium chlordane ..L R1 <>.:.f1" l~1 -----Chloride chlorobenzcne ----.....e:::: fr: sac1:Dr5 .. Chromium chloroform I ------__ Copper o-acsol > •lb e,i! <o, Jo ppm fluoride --m-crcsal ----p-crcsol __ UN72AAJL-< 0,40 Pf""'-Iron I I<. .-----Lead cresol __ ,hf DU, ~HtI,L</,0 Pf'M --1,4-dichlorobenzcne __ WX1tf .Q', <~.o,,,;t-__ Manganese --~ <tJ,iOp}) __ Mercury --1,2-dichloroethane I . -r <o., '¥'.em Nitrate 1,1-dichlaroethylene ----Selenium 2,4-dinitrotaluene ----heptachlor Silver --I Radiochemistry Sulfates hcxachlorobenzenc ----Zinc hcxachlorobutadiene ----Parameter Results (PCl/1) pH hcxachloroethanc __ Gross Alpha __ Conductivity --methyl ethyl ketone I --Gross Beta TDS nitrobenzcne -----pentachlorophenol TOC --pyridine I --Microbiology tetrachloraethylcoc ----__ trichloraethyleoe Parameter Results (Col/lOOml) --__ 2,4,5-trichloraphenol --I __ 2,4,6-trichlorophenol : --__ vinyl chloride --endrin --lindane Date Received l}P,9/ 5!i°1_ Reported by --methoxychlor --toxaphene :il·A P6S'f" ~ _q J -- I Dale Extracted Jl·/-'/1 ~ K"ffeate Reported 2,4-D --2,4,5-TP (Silvex) ~ 81'A C)1 ~fl''N --Dale Analvtc· ,;..f1 9-J.?A, -~ o I ah Numher . . "., l <. g N.C. Dcpanmcnl ol em,;ronmcnt, I lcalth, & Natural Resources SAMPLE ANALYSIS REQUEST n Solid W■SIC M1n1gcmcn1 Division C..L ~ c_ L ft State Labontory of Public Hcahh P.O. Box 28047, 306 N. Wilmington Street Ralcil,h, North Carolina 27611 .e Number 9 ':/ J) aoo 'is'I 3 . -5''] g Field Sample: Numbcr ____ :..,l, ... s'-'o~;_,J-:......._ ____ _ U . . ) +!-A~}j,JOO-? . p Name of s,tcC,-e.o C Sb I Q, -f (l {' l ;t ( ._5 fHi) rnL u.S,te Locat,o O L \6, rn Q l ! t I\ ) ) Collected By ./J (l ~ ~'t,g ALL" A I ID# ·7 /_; Date Collected '7 -/ I -CJ / D Agency: ' Hazardous Waste Solid Waste VSuperfund TCLP Compounds ---- Time 15·; 5 D Sample Type -Inorganic Compound! Results(mg/1) Environmental Concentrate Comments Arsenic -Barium ... " · g [: !'.'(.i ,. n _ Ground water (1) Solid (5) 1r' 1:;.h I -Cadmium u { }_i:J: \: ~ :1 ! ', -o :.:. _.,/ -Chromium _ Surface water (2) _ Liquid (6) VD e-; AN e 1 (c..t, s. 1 -Lead -n _ Soii (3) I l Mercury 0Ui ~;:t ~td Stt·:;J;., f, ..s T,(ls_:'t, £ ,S -Selenium _ Sludge (7) -Silver / Other (4).SfJ>rmf,0--Other (8) - I - I Organic Chemistry Inorganic Chemistry ' Parameter Results(mg/1) Parameter Raults(mg/l)(mg/kg) Organic Compounds Results(mg/1) v P&T:GC/MS Arsenic benzene ✓ Acid:B/N Ext. -Barium -carbon tetrachloride MTBE -Cadmium -chlordane ✓PC.. t3.:~ --<O,lO /!12."' Chloride chlorobenzene v Pqzyn,E-5 -Chromium -chloroform I --_Copper o-aesol -C:ndc'ifL <n,/D ,..,~-Fluoride -m-cresol --p-aesol I __}, iAl~AJJt-<"0,"fOF/'M,-Iron -_rr1r: ru DX;f::,,c HLl!fc 1,0 PIM'--' Lead . cresol _,oxe e1f£AJE-<;;)~ _Manganese -1,4-dichlorobenzcne -_Mercury 1,2-dichloroethane I ~ ': -b <O, v-'5 Nitrate -1,1-dichlorocthylenc j\(. 5 "T % ~do ,12/UH --Selenium 2,4-dinitrotoluene -= heptachlor Silver -I Radiochemistry Sulfates hexachlorobenzene ---··--Zinc hexachlorobutadiene -Parameter Results (PCl/1) _pH hexachloroethane -I _ Gross Alpha -Conductivity -methyl ethyl ketone -Gross Beta TDS nitrobenzcne --pentachlorophenol TOC -pyridine I -Microbiology -tetrachlorocthylene -_ trichloroethylene I Parameter Results (Col/lOOml) _2,4,5-trichlorophenol -_2,4,6-trichlorophenol vinyl chloride --endrin I -lindane Date Received 1, IJJ (j/ Dt1m Reported by -methoxychlor -lJM, -Ill-/1._sr(I llwf-3 Ji I -toxaphene • Dale Extracted 8-/·'1 /) ~.pip ~;§'i;P•tc Reported -2,4-D ~ s~11 -2,4,5-TP (Silvex) Date Analy: ~-!// g-.1.l-'lft3'9_ Lab Number ____ 91.ZG~~'.l} ' n n 0 0 I SOLID WASTE MANAGEHENT DIVISION SUPERFUND SECTION Chain of Custody Record Hazardous Waste Materials Location of Sampling: Generator --Treatment Facility =Disposal Facility CERCLA Transporter --Storage Facility --Landfill Other:---,-,,-,-~,.,,-,,--;:---------~~-~ (1 · ~ i-1-r-11./.-bu..XlD...b 1 •... • •8 , "H . n . Company's Name =<'.'..Of i1 fr · iroc•,+'.'t c, 5Au~elephone =--~·--f!:1 tff~ r •, n• 11J' Address PL !_ynourtt. ) Ld ~.s 1-fIJ\)('..,...-rn N (' Collector•s Name Ulu,J-t... 0~Qp~ Telephone: ' ~ignature Date sampled _ _,__-_,_~\_-_r~-1~\ _________ Time Sampled _______ _ Type of Process Generating Waste ------------------I Field Information: ________________________ _ I I I I I I I , I Field Sample No./.:5O1() /501/ f.'·--1)/ 2-1.5 (> l-3 1,501 '± ti le c1.ur.£;t: title signature title inclusive dates Results Reported: ~ P11t.UZ ~ignature ti.tle date Instructions: Complete all applicable information including signatures, and submit with analysis request forms. g /NEUTRAL ANO ACID EXTRACTABLES ll COlll'OONO ~-nitrosodimethvlamine ~2-ch loroethvl )ether loroohenol ohenol ~ ~ich lorobenzene -"i ch lorobenzene I -di ch 1 orobenzene ois{2-chloroi 1 )ether h ch loroethane ~ i troso~i -n...nr"f"Y'lv) dffli ne n i trobenzene i horone 2 it~henol 2.4-dimethvlohenol ~ ,{2-chloroethoxvlmethane -dichloroohenol I 4-trichlorobenzene n hthalene -~ achlorobutadiene 4 hloro-<n-cresol -hexachlorocvcl~ntadiene -trichlo=henol ronaohthalene acen•nhthvlene d. thvl ohthalate 2 -dinitrotoluene a n•nhthene 2 4-di ni troohenol -dinitrotoluene 4 itroohenol fluorene 1 hlo~henvlohenvlether thvl ohthalate 4 ,-dinitro..o-cresol f henvlamine ~ b<>nzene N>r<Y,henvlohenvlether hexachlorobenzene ltachloroohenol nanthrene anthracene lutvl ohtha late oranthene STATE L.'180RATORY Of PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. OEPARTIIENT Of fl.Jl1AH RESOURCES P.O. BOX 28047 -306 N. WIL"INGTON, ST., RALEIGH, N.C. 27611 ORGANIC OlE"ICAL ANALYSIS LAB NO ,_,1_J/ -,r_ .._, 1.11~:i. 7 c.•1..1..1~29 <II,}._/-.;;_9 FIELD I 1,-,,., I I I ,o/ ..l. / <;7J /, '? I \ol'I- TYPE { ' ri { -31 ( <.J. ' ( ..Ji UNITS .. "' /kal • .. n/ko ,.,-f un/ko -/kn1 ~ ''" ~ (,,(__. LA......, I .. ., ~ Sw ~"-~O /I}. 'f."tO .-:-oJ '-"O JO/ ao "' -~O ., ~,., '-I' /ti ,_,"O /ti) 'l'Jl) so1/1 • ..-n IA/ ,,,., ~ / . . \ , .. , ' \ ' ml>L I Estimated value. H,.o/S0/1- Actual value is known to be less than value given. ( l .. n/j .. n/ko · :1 • e , r. 1.1 ;; i .. _,_.,,-_ ·~ ' · . .. . :·1 ,• t ·1 1. I i ~ : , l l,' I.; ......... ...,,. ~ ~ Actual value is known to be greater than value given. , llaterial was analyzed for but not detected. The nunber Not analyzed. is the tlininun Detection Limit. m'JJL ..:. --- Tentative identification. On NROC List of Priority Pollutants. •;a. D-tv.{.f.)-tOn 06 Heai..th SVtv-tce.6 T 3068-0 (4/86 Laboll.ll.to~yl { l .. n/ 1 un/ko ~ .. ' ' ., .... . ' I .. ...... H STATE LABORATORY Of f'IJBi.lC iU:AllH DIVISION Of HEALIH SERVICES, N.C. 0£PAIHIIENT Of fUt\AH RESOUHCES P.O. BOX 28041 -306 N. WILNINGTOH, ST., RALEIGH, N.C. 27611 I ORGANIC OlENICAL ANALYSIS BASE/NEUTRAL ANO ACID LAB NO C//.?I •I Q/,J.t.,.J, :t::)/"'J ~o c./ / ~ /....::1~ EXTRACTABLES FIELD# /~I/ I \-0/~ I I l7'11::? I ri ft.I CONPOONO TYPE I~ l r 31 ' I <i l ( . '.J i I UNITS ---',V ua/kn -a un/ka' .. / /kn --.L.I, ~n71(a' ~vrene in/""" vC . I cA...:: /.1,._ - ' ,l)nzidine S'O ,,. butvl benzvl ohthalate J0/'1'10 ~i\~ \i..l nz (alanthracene hrvsene .. 3.3--dichlorooenzidine S-fJ) _, P• i s(2-<>thvlhexvl l ohtha late IA/ I "'"' >:iHJ i..,i-octvl ohthalate 10/.J_:?o benzo(bl fluoranthene ro•·· f nzolkl fluoranthene nzo (a) nvrene denoll 2 3-<:dlovrene dibenzo(a hlanthracene . -, nzo(a h i l=rvlene ' , .. I I I niline <,o/Jl,,"1, IA--(,L., A , L,L- 1&anzoic acid ,enzvl alcohol 4-<:hloroani I ine ... ,,, nzofuran ,Ul '=>11 thvln•nnthalene 2--<nethvl"""""I ~thvl"""""I .. , troani I ine . ..-01.J t..,;o 3-ni troani 1 ine -itroaniline ·, . . .4 5-trichloroohenol ~, I / ·~ ■ mnL 11:1 -Estimated value. Ha.0/ SD/I... K -Actual value is known to be less than value given. ( l ( I un/ I un/ka ""/1 ··•/ka I -.. ., ,. " ' a . ir r. ~·11, ' ' ' .,I . -. ' .. ~~11r111 -.;1-r.1• !fl I-Actual value is known to be greater than value given. -Material was analyzed far but not detected. The numer NA -Nat analyzed. is th•? Nin irrun Detect ion Limit. -Tentative identification. fl -On NROC List of Priority Pollutants. Iii. C. D-i.v-i..6-i.un o 6 Heo.Uli Svr.v-i.cu ~HS 3068-0 l4/86 Lo.boll.a.-to~y) R '-Laboratory No. N. C. OEPARTIENT OF ENVIAONIEIIT, HEALi[H, & NAT~L RES<UICES DIVISION Of LASORATalY SERVICES, EHVIRONIEHTAL SCIENCES SECTION P .0. BOX 28041 -306 N. WlUIINGTON Si[, RALEIGI, N.C. 27611 f/,j &J,-f PI.IIGEAIILE !Xlll'aiNOS Date of Analysis D m I I .. I I I I I I I , I 1r\ p r.,1 ;:.,,',~ COIIPOUNO Dichlorodifluoranethane Ch 1 oranethane ,(Yinvl Chloride Brarunethane Chloroethane Trichlorofluoranethane ✓1-1-0ichloroethvlene llethvlene Chloride tert-&tvl llethvl Ether trans-1-2-0ich loroethvlene I•-r-··1 ether 1 1-0ichloroethane 2 2-0ichlo ne cis-1 2-0ichloroethvlene Chlorofonn /BOO Bramch loranethane ✓1 1 I-Trichloroethane 1 1-0ichlor ne ✓Carbon Tetrachloride ✓Benzene ✓1 2-0ichloroethane ✓Tri ch loroethv 1 ene 1 2-0ichlo ne Brarodichloranethane Dibrmonethane Toluene 1 1 2-Trichloroethane Tetrachloroethvlene 1-3-0ichlo, ne Oibrarochloranethane 1 2-0ibraooethane IEOBl 1 ~h 1 orohexane ,:I , 1.... -l ___ L __ ., l IDl£NTS: 119/l I I I ''""Le- A ..J.,..,.. /I.,. . 11g/l ==-=-==-=---====!==--.,;=== _:Chlorcbenzene · 1 IEthvlbenzene , 1.1.1 2-Tetrachloroetha= .n. ~ ~I .. ~""''·" ,, J·>-xv 1 ene \! \~ 1-""' 1 ~-= ~ \J' ~-.-. .-...:,, _Ji.-Xvlene ;:,...Xvlene ', 1-·· I _Stvrene _!!ranofonn ~"'' , _,._ IJ.JI• I lbenzene 1. 1 2 2-Tetrachloroethane l!ranobenzene -2•-l'-··lbenzene ,1 2 3-Trichlo -ne ~2-Chlorotoluene 1 3 5-Trinethvlbenzene 'I-Ch lorotoluene _tert-&tvl Benzene ?entachloroethane 1 2 4-Trinethvlbenzene sec-&tvl Benzene _J)-I ltoluene 1. 3-0 i ch 1 orol>enzene tl 4-0ichlorol>enzene _n-&tvlbenzene 1.2-0ichlorcbenzene Jais 12-Chloroi 11 Ether _ 1. 2-0 i bra,o-3-Ch 1 O• ne _:1.2 4-Trichlorol>enzene 1-lexach lorobutadiene _,1.2 3-Trichlorol>enzene ____________ _._ ____ _ llllL -llininun Detection Limit for water (EPA llethod 502.2), is 1.0 11g/l. J -Estimated value. K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. U -llater1al was analyzed for but not detected. NA -Not analyzed. 1/ -Tentative identification. ✓ -Re~ulated voe T -Tr1halarethane N.C. Dept. of Environnent, Health, & Natural Resources DEHNR 3068-0 (Rev. 1/91 Laboratory Services) 0 '- STATE LABORAIOOY Of f'U~L!C HEAL IH DIVISION Of HEALTH SERVICES, N.C. OEP,'.RTIIENT Of HUIIAH REICXJRCES P.O. BOX 28041 -306 N. IIILMINGTON, Sl., RALEIGH, N.C. 21611 IJRGAHIC MMICAL AHALYSIS II PURGEASLE CD'IPOJHDS a,-2,u,:-iq IJ -----------+...!:..!.~...!..-.j-1.:.Ll.cl..J'-'----!--.!..>L~e!=--f---"--"'-';":-"'-t--"16._,0SI':-' '"'L:--+---:--:---t--,------,----- LAB NO q,').l,11. Q/:7ln2f q12u ,'fi' FIELD I ,.5011 1501;,._ J5oJ3 II ch I or~thane bratarethane II dichlorodifluoranelhane IJ vinvl chloride ch loroethane melhvlene chloride 11 lrich lorofluoranethane IJ ethene. 1 1-dichloro ethane. 1 1--dichloro- I 1 2-trans-dichloroethene chlorofonn ethane 1 2-dichloro-- I ethane, 1 1.1-lrichloro-- carbonlelrachloride brorodichloranethane · prc,,ane. 1 2-dichloro-- I 1 3-lrans-dichlo, trichloroethvlene chlorodibrmorethane nzene hane, I I .2-trichloro-- .3-cis-dichlo ne 2-chloroethvl vinvl ether I bron:ifonn ethane, 1. 1.2.2-tetrachloro- ethene. tetrachloro- I toluene ch lorobenzene elhvlbenzene I acetone 2-bulanone cart>ondi sulfide 12-hexanone 4-<tethvl-2~ntanone stvrene I vinvl acetate xvlenes f+otal) TYPE UH ITS 10--b ,I, 5 --L.. , 10 -L in' ,; I ,o ,o !', ( .3 l (."3 } I ,1 l { '-/l I l I \ un/ l('uo/ko uo/1 un/1 ,<.;;"/kn un/1 ""'""' un/1 un/ka ..n/1 ""/ko I' , , ,. I J _' • 1-j •f! • i,'. \_l j. I _-.,. \1 ~ •"' _\JtL.s V ! .L;., I-... i . . . -' •\ . . . ·, . ' ' / . , / I ---------+1"°,;;nsv1,11cr-,_t.+-----+----1----+-----1-----t----- I J -Est 1mated value. K -Aclual value is known to be less than value given. L -Actua~ value· 1s known to be greater than value given. ft -llaleria l was analyzed for but not detected. The nurber -Not analyzed. -Tentative identification. , -On NROC List of Priority Pollutants. C -:'.i4~P/;c:, LAB <:.aNTAl'11NATION. ,1 N.C. Division of Health Services '/ DIIS 3068-0 (4/86 Laboratory) is th" Minin,,n Detection Limit. D "-0 I I I I _SOLID WASTE MANAGEM,ENT DIVIS I~, 'EIVtU SUPERFUND SECTION n1:.v CERCLA' Chain of Custody Record GCT l c l~S! Hazardous waste Materials SUPERFUNDSECT/ON Location of sampling: Generator Transocrter --Storage Facility Company's Treatment Facility =Disposal Facility Other: --Landfill -i\ It 'R.!i:t D l Name i;eoc~B: -R.ie'ifl e. -SAi<'<iliLLTelephone: __ _ Addressi-P--""~P--l.l.LS~-½t--,-~L~l)"---R!¥,;~:I.~1~~~t-2.~=--:I_0:::...,_~~1_~c=.2-.:------- Collector's Name Telephone: 9 I 9 '133-e<''?D I Date sampled ___ 1___,_-_1~\~--9,_I ________ Time Sampled ______ _ Type of Process Generating waste _________________ _ Field Information: ________________________ _ I Field sample No./6 303 ll3D4 /{,3()!5 I{, W0 I I I I I I , I t:iitle 12 3v{fe~ inclus1etes signature title inclusive dates Resu1t7_yepprted: dpf? ;;; /tZ/£ . signature q t?cft( date Instructions: Complete all applicable information including signatures, and submit with analysis request forms. I N.C. Depanmcn, o( Environmca~ SAMPLE ANALYSIS REQUEST I lcallh, & Natural Ri:sourtcs "Solid Was1e Manag<mcnt Oivili011 ('. .. L ,'\C.,. L fr State l.abontcuy of PUblic Hcallh P.0,..!!,1-llf4'UI Wf'1il'fafOn Stn:e1 nL~1iv .. ~--''"'"' 21611 'Number(j':f.J) 000 '8'13 .-5']2, FieldSampleNumber /{pJtf.&T 1 1 ~ 199l 0 . . . ) +l-fl/{ljJOO~ .· . p . ~uptotllllB C:tl'·~ Name of S,tc{'-,-e.pc~, a, .(n,r i ;ti<' ..SA-y) tnrL!Stte Locatmn_ L ~rn QI l t ~ 'm»'-9'"''i~r:,,, (' 0. ) J ' ECoilected By .JJ H 6 ~'E.g Ii l L f A I ID# ·7 l,e Date Collected '7 -II -q / Ttme IQ.' '-/ 5 Agency: Hazardous Waste Solid Waste i,/supc,fund TCLP Compounds -- I Sample Type Inorganic Compounm Results(mg/1) Environmental Concentrate Comments / Arsenic 9,· 01:: /Barium ,QQ 1--Ground water (1) Solid (.5) ,-!S tl~5 -QI ./Cadmium < a, o 8. _r,<J D~i;,./l-ui:C.. /Chromium < (2,/ Q __ Surface water (2) Liquid (6) zs.S 0 m1_ /uad ( D., .s.-o IL soil (3) /Mercury <'a,o?-Sludge (7) ~ Selenium <o.oo / Silver s'.'.Q, /Q -- 1 1-Other (4) Other (8) --I I ----Organic Chemistry Inorganic Chemistry -- I ~ Parameter Ruults(mg/1) Parameter Raul ts (111allHmg/kg) Organic Compounm Results(mg/1) _P&T:GC/MS V Arsenic J:2:,, benzene LBarium --Acid:B/N Ext. ::')ds 0 carbon tetrachloride --MTBE _L' Cadmium L... 3o chlordane ----Chloride chlorobenzene ----I ✓Chromium --':Jo chloroform -- --__ Copper o-acsol --Fluoride m-cresol ----=p-acsol I --Iron --__JLL-Cad II,.., cresol ----Manganese --1,4-dichlorobenzcne I --✓Mercwy .L...Q-c:l --1,2-dichloroethane --Nitrate 1,1-dichlorocthylene v Selenium --< /, l-· 2,4-dinitrotoluene ' ::::Z-silver = heptachlor .,__ 3Q I Radiochemistry Sulfates hcxachlorobenzcne ----Zinc hcxachlorobutadiene ----Parameter Results (PCl/1) hexachloroethane pH I --_ Gross Alpha __ Conductivity methyl ethyl ketone --Gross Bela TDS nitrobcnzcne -----pentachlorqphcnol TOC -- I pyridine --Microbiology tetrachlorocthylene ----trichlorocthylenc Results (Col/lOOml) ----2,4,5-trichlorophenol I Parameter --2,4,6-trichlorophenol ----__ vinyl chloride ---endrin --lindane Dale Received Reported by = methoxychlor --toxapbene I Date Extracted Datl)R~rted 2,4-D I' 569 JOL12~1 --2,4,5-TP (Silvex) --n .. ,_ ",....,1,~ .... 1 l '"'h Nurnhrr D N.C. Dcpanment ol Environm••~ SAMPLE ANALYSIS REQUEST ~~•-•11!'1\11184"11 ol Public Hcahh I Jcahh, & Natural Resources I \lliilV~ 116ilcAvi1mington Street id Wute Ma .. gcmcnt Divilion (1 z.. 0 C,_ L ff Raleiah, Nonb Caroli .. 21611 -'\. · uCT 1 ~ 1991 e Number 9 :f J) DO O 3'.13 -59 2, Field Sample Number $Ut~~s'ro~ 11 . . ) . . #-FtR}j,.)00~ .· . p h 11 Name or S11e(.,..e.p C Sb I Q, -lac I t: C ..Sfty) mrus,te Locatton L :2:, rn O I I IA -S b ', n €:,IDG {' 0. ) ) • Collected By .1.J A '5 k'[_8) ALL F A I ID# ·1 /..e Date Collecti:d '7 -I / -9 / Time / 0: ::J. 0 Agency: __ Hazardous Waste __ Solid Waste i/'superfund TCLP Compounds I Sample Type Environmental Conaentrate I-Ground water (1) _ Surface water (2) I _Lsoil (3) 1-Olher (4) _ Solid (5) 11.:..C-""""'E,_-__.0'--'I'--~~~-~.,....,. ::;::i) D 1\(:,11 <..J.J'-'-I liquid (6) ao o m t_ Sludge (7) __________ _ Other (8) __________ _ Organic Chemistry RHult.s(mg/1) Parameter P&T:GC/MS -Acid:B/N Ext. ____ _ MTBE Inorganic Chemistry Parameter / Arsenic ~- ~rium Resuluc:rg(mg/k&) 30 ✓Cadmium -Chloride ...:::::-Chromium _Copper Fluoride Iron &-a,o 7uad .J.o _Manganese /Mercury ""-.o _ c::, --Nitrate ~Selenium ( /, 0 1----------------1 2Silvcr ..,_ a,o Radiochemistry Sulfates Zinc pH -Conductivity ______ _ Parameter _ Gross Alpha _____ _ Resulu (PCl/1) Gross Beta TDS TOC Microbiology Results (Col/lOOml) Date Received ________ Reported by ________ _ I Dale Extraclcu _____ Dal'tJt':'J310 JU[ 12 91 ,..... , • I 1 "},, 11, I,..-I,,. - Inorganic Compounds _LArsenic ..L. Barium _LCadmium L Chromium Luad __..::::Mercury ~clenium i/ Silver Orpnlc Compounds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-aesol m-cresol --p-cresol -cresol Results(mg/1) Q.Q,~ < o. 0 8 ( Q. IQ (o. /o Results(mg/1) ------ 1,4-dichlorobenzene ---''---- 1,2-dichloroethane 1,1-dichloroethylene _____ _ 2,4-dinitrotoluene = heptachlor hexachlorobenzene hexachlorobutadiene _____ _ hexachloroethane methyl ethyl ketone _____ _ nitrobenzene -pentachlorophenol -pyridine · tetrachloroethylene trichloroethylene -2,4,5-trichlorophenol _____ _ -2,4,6-trichlorophenol _____ _ --vinyl chloride --endrin lindane = methoxychlor toxaphene --2,4-D 2,4,5-TP (Silvex) D N.C. Dcpan..,.nt of Environm••~ SAMPLE ANALYSIS REQUEST State Laboratory of Public Health i llcallh, & Natun.1 Re.source& P.O. Bo1 28047, 306 N. Wilmington Street ~lid Wutc Management Divi■ion (!_2:. ~-('.,. L ft R.llciib, North Carolina 27611 .. e Number 9 4 J) a O Q a I 3 ...5 '] 2, Field Sample Number tittililV t:.U II . . ) . +t-AR,:t:IJOO~ . . p . t I G' . \j ' 100~ IJNameofS,tc{',-e.nc<e:,•Q, .{·aci±:lc ~A;µ)mrLLSttelocallon Lk'?,rnn11, \ L-1!.u-S-b(n IDt'--. (' o. ) ~ ' . I Collected By .JJ Ad~'E.g /ilLf A) JD# ·7 y Date Collected '7-I I -qSU ERfUftl~CTl')N:.</5 Agency: Hazardous Waste Solid Waste /supcrfund TCLP Compounds -- I Sample Type Inorganic Compounds .. Resulu(mg/1) Environmental Conc:entral~ Comments ~Arsenic S::a-n1 I-Ground water (1) -..L:Barium a, !i a Solid (5) /...f.d rYlB b -[) I LCadmium < '2-08_ IAJ D f<.6.(M.iJ:Z5 ,/Chromium ( '2· I 0 _ Surface water (2) _ Liquid (6) a~n O'.l k ~ad ~0--'> 0 I _soil (3) _u,Mercury Q,Q:2 Sludge (7) ?'Selenium <O-QQ_.i- Silver (0./Q JL'.. Other ( 4)5E.h,..7l\£...rc._ Other (8) -- I ------ I Organic Chemistry Inorganic Chemistry -- Parameter Resulu(mg/1) Parameter lwullli (JJia/1) (mg/kg) Organic Compounds Ruults(mg/1) P&T:GC/MS / Arsenic <2.,a__ benzene --Acid:B/N fut. ✓ Barium J,7 carbon tetrachloride --MTBE _u:::Cadmium .L..' '.:') chlordane ---Chloride chlorobenzcne ---I -~Chromium ~ d,C:, chloroform ---__ Copper o-aesol --Fluoride m-cresol -----p•crcsol I -Iron --;:71.ead a,1 cresol ---__ Manganese --1,4-dichlorobenzcne I -....t::::'.'Mercury .L..o,) --1,2-dichloroethanc -Nitrate 1,1-dichloroethylene < l, ei --7selenium 2,4-dinitrotoluene ilver -1...a_o --heptachlor I Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Resulu (PCl/1) hexachloroethane _pH --I _ Gross Alpha __ Conductivity methyl ethyl ketone ---Gross Beta TDS nitrobenzcne --= pentachlorqphenol TOC --__ pyridine I --Microbiology tetrachlorocthylene ----__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol I --__ 2,4,6-trichlorophenol ---__ vinyl chloride ---endrin --lindane Date Received Reported by = methoxychlor __ toxaphene I Dale Extracted Da\9f~ff~ , 11 II 12(n 2,4-D = 2,4,5-TP (Silvex) n ' ' , t,. I., .. 1 " - H N.C. Dcp1nmcn1 o/ Environm••~ SAMPLE ANALYSIS REQUEST Stile labontory o/ Public Heallh llcallh, & Natural Resources P.O. Box i8EJ.\ft_l\ 'flmington Street ~lid w .... M1n11emen1 Division (:!..L ~ c~ L ~ t< I:,(.; c,~ C.rolina 27611 .. e Number Cf::{ J) 00 0 SI 3 ..59 3, Field Sample Number l[IR. p'.0.'f'.191:!1 D . , +¼-l't~)J._)QO.b . p . Name of Sitcf1te.ocn 1 o, .{ QC J :\:11'.' --lfik > rnr LtSite Location L \6,rn Q J SIJl>Ei~fHtil0~U\ON'.)J:Or:,,, C' O. :::.J ) ' R Collected By .LJ A rs k'E{_j ALL F 6 I ID# ·7 Le Date Collecti:d '7 -1 I -q I Time 1 ,;J .' 1 .:5 Agency: Hazardous Waste __ Solid Waste v'superfund TCLP Compounds -- I Sample Type ln.'.'.'.:nlc Compound,, Results(mg/1) Environmental Concentrate Commenti Arsenic Q.o r 1--Ground water (!) ,7Barium o. 6 ~ Solid (5) ,u::z::i-o I ~ Cadmium ~ Q-~ d .!.. >J u /\Ca, II-~ ~ Chromium s: 0, (Q __ Surface water (2) _ Liquid (6). ,:J.,.£!i n m L__ ___k::'Lead ~0-.!,-c) m _ Soil (3) ...---Mercury ¾lenium a,a-;;i _ Sludge (7) 0,0Q.C Silver ~ Q. (~ I _L Other (4) otJmnlJJT Other (8) I Organic Chemistry Inorganic Chemistry Parameter Re,ults(mg/1) Parameter ResullsuPl/f) (iiog/kg) Organic Compound, Re,ults(mg/1) P&T:GC/MS v Arsenic q.g benzene --Acid:B/N Ext. ..JLBarium '.:l5 carbon tetrachloride --MTBE ~admium \tao chlordane ----Chloride chlorobenzenc ,,/Chromium --I -~,;>,o chloroform ---__ Copper o-cresol --Fluoride m•crcsol --- I -Iron p-cresol VLcad ~o cresol -------__ Manganese --1,4-dichlorobenzcne -✓Mercury L..o -\ --1,2-dichloroelhane I --Nitrate 1,1-dichloroethylene < /, ;'.) --~Selenium 2,4-dinilrotoluene Silver -"--iz,O __ heptachlor I Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobuladiene Parameler Results (PCl/1) ----hexachloroethane pH I _ Gross Alpha __ Conductivity = methyl ethyl kelone -Gross Bela TDS nitrobcnzcne --= pentachlorophenol TOC --__ pyridine I --Microbiology lelrachloroethylene = trichloroethylene --Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol I --2,4,6-lrichloropheool ---= vinyl chloride --endrin --lindane Dale Received Reported by __ methoxychlor __ toxaphene I Date Extracted Date Reported __ 2,4-D U I 35l2 JUL 12~ I _ 2,4,5-TP (Silvcx) Oatr, A nalvtt·rl I ah Num er -·--·- I ,, I ,, I ' ' '-I m I I I I I DATA ANALY1:ED BY IEA I See Volume II ID I I I I I I I , I _',. •, .... -. .. 'I i::,.Liiihthou~e(CJ , phic Maps; Plymouth SOURCE: USGS Topogra West., G Light th East N.C., C 1979; Pymou ' N •• , C 1979; WestO\ler, N.C.,1954 1954; Woodard, N. ·• 0S1ump DRAWN CHECKED SHEET DATE JOB No. , / ' . s \ 200() ,u: FILE No.