NCD000770487_19980901_Johnson Controls Battery Group_SERB PA SI_Expanded Site Inspection - Appendix B-OCR

I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
STATE OF
NORTH CAROLINA
Department of Environment
and Natural Resources
Division of Waste Management
Superfund Section
EXPANDED SITE INSPECTION
APPENDIX B
Johnson Controls -Globe Battery Division
NCD 000 770 487 I
Winston -Salem, Forsyth County, Norlh , arolina
Reference No. 02549
September 1998
Doug Moore
Environmental Chemist
Division of Waste Management
Superfund Section
I ,
I
I
I
I
I
I
It
I
I
J ly 28, 1998
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
REGION~
SCIENCE AND ECOSYSTEM SUPPORT DIVISION
OFFICE OF QUALITY[ASSURANCE
I 980 COLLEGE STATION RD
I A THENS, GA 30605-2720
I
JUL ;:, .l 1:1:18
SUPE!iru1,u vt:Vf/ON
M [· Doug Moore
North Carolina Department of Health, Environment and Natural Resources
suferfund Section
40\ Oberlan Road, Suite 150
Raleigh, North Carolina .
De r Mr Moore:
Enclosed is the inorganic and organic forms that you requested for Johnson Control Globe,
cas6 no. 25633, project no. 97-378.
If ybu have any questions or if I may be of further assistance, please contact me at 706/355-1 862.
Sin erely,
.~'M-._h~~
~A. Guthrie, P.E.
I E,er,m~bl E,~,-
Enclosure
I
It
I
a
u
u
m
I
I ,
I
I
I
I
I
I
It
I
I
a. Syste111 Monitoi/ing Co11npou11d Su1n111ary
(For1n II V()A)
JS<o35
q7/ 03;1 ~
. . I)LL-0 ;;)...-:£,])&.
22
I
I
I
I
0
0 ,
I
I
I
I
'9
I
I
2A I WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name: COMPUCHEM ENV. CORP. Contract: 68D50004
SAS No.: Lab Code: COMPU Case No. : 25633 SDG No. : DLL02
page OJ.. o£ 01
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
s
s
EPA SMCl SMC2 ISMC3
SAMPLE NO. (TOL) # (BFB) # (DCE)#
I ------------:::===== ====== :::=====
VBLKMM 102 100 95
DMH91 102 102 98
DMH92 109 108 105
DMH94 98 96 95
VBLKTG 105 104 100
DMH95 104 104 99
DMH97 102 101 100
DMH99 105 104 102
DMJ0l 107 108 105
DMK06 109 109 104
VBLKXG 104 100 97
DMK09 102 100 98
DMKll 102 100 100
DMK13 96 94 94
DMP51 102 99 98
DMP52 104 102 102
DMP57 105 102 102
DMP59 103 100 103
DMP61 105 102 102
DMK13MS 95 93 99
DMK13MSD 101 96 107
VBLKYY 89 86 84
DLL02 91 90 88
DLL05 89 88 85
DLL06 89 88 86
VBLKQA 100 98 95
VHBLKG7 97 96 93
I
I
QC
MCI (TOL) = Toluene-dB
MC2 (BFB) = Bromofluorobenzene
OTHER TOT
OUT
::;;;::::::::::;;:;: ---
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
--
--
LIMITS
(88-110)
(86-115)
SMC3 (DCE) = 1,2-Dichloroethane1d4 (76-114)
# Column to be used to flag recovery values
* Values outside of contract reJired QC limits
FORM II VOA-1 OLM03.0
23
I
-a. Surrogate Percent Recovery Summary
I
I ~ ~-(Form II SV)
I JO~
~ I ~s;tp-33 ~ • Cf1'0~uY
D l 9&.
I ,
D
I
I -
~ "'I:.
I
I
! I
" --: -
I
I 285
I
'9
1
I
I
I
D
D ,
I
I
I
I
I,
I
I
2C
WATER SEMIVOLATILE I SURROGATE RE~OVERY
Lab Name: CompuChem Env. Corp. I Contract: 68D50004
Lab
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
Code: COMPU Case No.: 25633 SAS No.: SDG No.: DLL02
EPA Sl S2 S3 S4 I S5 S6 S7 SB ~PLE NO. (NEZ)# (FBP) # (TPH)# (PHL)# (2FP) # (TEP)# (2CP) # (DCB)# ============ ::===== ====== ====== ===:::== ====== ======= ====== ====== SBLKTG
DMH91
DMH95
DMH97
DMH99
DMJ0l
DMK06
DMK09
DMH92
DMKll
DLL05
DLL06
DLL02
DMH94
SBLKTH
DMK13
DMK13MS
DMK13MSD
DMP52
DMP57
DMP51
DMP61
DMP59
-~ "'
66 64 87 72 77 76 76 56 65 66 117 67 63 95 68 49 72 72 100 72 74 86 80 58 60 61 91 65 63 76 68 52 67 68 94 72 74 81 77 64 64 65 93 68 67 79 74 54 62 63 85 67 67 75 72 53 36 34* 44 36 34 41 37 28 78 81 117 85 86 98 90 68 79 81 113 84 74 95 90 66 61 66 98 65 65 76 70 49 68 65 106 67 71 82 73 52
62 62 99 62 59 75 69 50 73 80 95 80 83 78 83 64 47 49 111 52 55 76 54 39 71 so 103 84 83 90 86 64 69 71 111 72 67 94 74 54 70 74 113 84 80 99 86 60 87 84 112 86 93 98 95 76 61 66 105 72 68 91 73 55 87 92 112 97 98 106 101 78 81 85 120 87 88 90 93 71
83 85 126 88 88 100 93 72
I • I
I
I
I
I . -
QC LIMITS
Sl (NEZ) = Nitrobenzene-d5 (35-114)
S2 (FBP) = 2-Fluorobiphenyl (43-116)
S3 (TPH) = Terphenyl-dl4 (33-141)
S4 (PHL) = Phenol-d5 (10-110)
S5 (2FP) = 2-Fluorophenol (21-110) ' S6 (TEP) = 2,4,6-Tribromophenol (10-123)
S7 (2CP) = 2-Chlorophenol-d4 (33-110) (advisory) SB (DCB) = l,2-Dichlorobenzene-d4 (16-110) (advisory)
I # Column to be used to flag recov~ry values
* Values outside of contract required QC limits
D Surrogate diluted out
TOT
OUT
---
0
0
0
0
0
u
0
l
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
-
-
-
-
-
1 __ 1
page or-01' 01 FORM II SV-1 OLM03.0
286
I
It
I
I
I
I
I
I
I ,
I
I
I
I
I
I
It
I
I
a. Syste111 Mo11itori . .1g Con1pou11d Su1n111ary
(F or111 II \rC)A)
22 ·
I
It
I
0
D
I
I
I
I
It
I
I
2B I
SOIL VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Mo= , CDMeCTCHCM SNV, mR,, CoocmJ
1
, SSDSOOM
Lab Code: COMPU Case No.: 25633 SAS No.: SDG No.: DMP60
Level: (low/med) LO w
page QJ., af 01
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
EPA
SAMPLE NO.
------------
VBLKX3
DMP64
DMP70
DMP71
DMP72
DMP74
DMP75
DMP64MS
VBLKYl
DMP65
DMP66
DMP67
DMP73
DMP64MSD
VBLKW6
DMP60
DMP62
DMP77
DMP78
DMP81
VBLKDl
DMP76
VBLKLl
VHBLKX3
SMCl SMC2
(TOL) # (BFB)#
====== ======
86 83
101 105
92 84
92 86
87 100
96 107
97 101
88 96
96 89
102 94
96 88
104 97
98 90
108 110
87 83
100 95
98 92
104 99
94 92
104 100
92 86
93 90
100 91
102 92
MCl (TOL) = Toluene-dB
\SMC3
(1DCE) #
j=====
83
110
92
95
98
117
113
101
105
106
103
110
105
117
I 92
i08
h.06
' ll0
106
115
197
102 ioo
]02
I
I
I
I
I
I
QC s
s MC2 (BFB) = Bromofluorobenzene
OTIIER TOT
OUT
=:c:==== ===
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
--
--
--
--
--
--
LIMITS
( 84-138)
(59-113)
SMC3 (DCE) = 1, 2-Dichloroethane-d4 (70-121)
I # Column to be used to flag recovery values
* Values outside of contract r~quJred QC limits
FORM II VOA-2 OL."103. 0
23
I
It
I
I
I
I
I
•
I ,
•
I
a
D
D
: 0
I
'e
l
I
a. Surrogate Percent Recovery Summary
(Form II SV)
346
I
It
I
I
I
I
I
g
I ,
g
0
D
u
u
I
2D
SOIL SEMIVOLATILE SURROGATE RECOVERY
Lab Name: COMPUCHEM ENV. CORP. Contract: 6BD50004
Lab Code: COMPU
Level: (low/med) LOW
Case No. : 25633 SAS No. : SDG No . : BMPml
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
EPA Sl S2 S3 S4 S5 S6 S7 SB
SAMPLE NO. (NBZ) # (FBP)# (TPH) # (PHL) # ( 2FP) # (TBP) # ( 2CP) # (DCB)# ============ ===:::::== ====== ====== ====== ====== ====== ====== ======
SBLKRS 26 26* 33 25 21* 26 26 24
DMP64 57 49 61 53 53 51 54 50
DMP64MS 50 49 52 49 49 46 ·51 46
DMP64MSD 53 49 58 50 50 46 52 47
DMP65 52 50 60 48 47 52 48 44
DMP72 32 32 36 31 28 29 29 26
SBLKRR 56 53 70 53 52 49 54 50
DMP60 53 51 60 53 51 50 53 45
DMP6~. 51 50 •• 57 50 50 47 5l.."' .. 44
DMP65RE 47 46 61 45 45 · 51 45 43
DMP67 39 35 53 36 36 43 36 35
DMP70 36 32 44 34 34 38 34 33
DMP75 30 28* 33 29 28 29 29 27
DMP76 40 36 38 38 38 37 39 36
DMP77 44 40 54 41 40 35 42 41
DMP78 28 25* 36 27 26 29 27 26
DMP76DL 29 26D 31 29 28 24 28 26
SBLKZV 52 47 65 51 47 48 51 44
DMP66 67 61 78 66 62 55 66 55 DMP73 49 43 53 48 48 45 49 40
DMP74 32 29* 54 32 29 42 30 24
SBLKAG 46 39 75 42 42 44 42 37
DMP71 54 47 62 54 54 54 56 39
QC LIMITS
Sl (NBZ) Nitro'benzene-d5 (23-120)
S2 (FBP) 2-Fluorobiphenyl (30-115)
S3 (TPH) ; Terphenyl-dl4 (18-137)
S4 (PHL) ; Phenol-d5 (24-113)
S5 (2FP) 2-Fluorophenol (25-121)
S6 (TBP) ; 2,4,6-Tribromophenol · (19-122)
S7 (2CP) ; 2-Chlorophenol-d4 (20-130) (advisory)
SB (DCB) ; l,2-Dichlorobenzene-d4 ( 20-13 0) (advjsfl"Y)
# Column to be used to flag recovery values
* Values outside of contract required QC limits
D Surrogate diluted out
TOT
OUT
---
2
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
1
0
0
--
-
--
--
-
--
--
page 01 of 01 FORM II SV-2 OLM03.0
347
I
It
I
I
I
I
I
•
I ,
D
0
D
I
m
•
" I
I
'
a. Sys_te1n Mo11itoring Co1npou11d Su1111nary
-(F or111 II V() A)
21
I
It
I
I
I
I
I
•
I ,
I
0
D
I
I
I
'-I
I
2A
WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Contract: 68D50004
SAS No.: SDG No.: DMP63
page 01 of 01
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
EPA
SAMPLE NO.
------------
VBLKXG
DMP63
DMP68
DMP69
VBLKTA
DMP80
VBLKYY
DMP79
DMP79MS
DMP79MSD
DMP98
VBLKTJ
VHBLKV5
SMCl SMC2
(TOL)# (BFB)#
====== ======
104 100
105 103
100 98
103 100
110 107
106 104
89 86
89 87
88 87
89 90
93 93
106 104
110 110
SMC3 OTIIBR TOT
(DCE) # OUT
====== ====== ---
97 0
103 0
102 0
104 0
113 0
107 0
84 0
85 0
86 0
84 0
86 0
100 0
107 0
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
QC LIMITS
SMCl
SMC2
SMC3
(TOL) =
(BFB)
(DCE)
Toluene-dB
Bromofluorobenzene
l,2-Dichloroethane-d4
( 88-110)
(86-115)
(76-114)
# Column to be used to flag recovery values
* Values outside of contract required QC limits
FORM II VOA-1 OLM03.0
22.··
I
It
I
I
I
I
I
I
u ,
D
I
I
I
I
I
It
I
I
-----
, !
a. Sys_tem Mo11itoring Con1pou11d Su111111ary
-(For111 II \T()A)
~S-0 33
q_1✓03;;;,?
"L--L--o 3 Sr£: J/
38
I
'9
I
I
I
I
I
0
u
I
2B
SOIL VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name: COMPUCHEM ENV. CORP. Contract: 68D50004
SAS No.: Lab Code: COMPU
Level: (low/med) LOW
Case No. : 25633 SDG No. : DLL03
~ i
page 01 of 01
EPA SMCl SMC2 SMC3 OTHER TOT
SAMPLE NO. (TOL)# (BFB) # (DCE)# OUT
=======-==== ====== =====;;: ====== ====== ---
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
VBLKV9-
DMH89
DMH90
DMH93
DMH96
DMH98
DMJ00
DMJ02
DMK07
DMK0S
DMKl0
DMH89MS
DMH89MSD
VBLKW5
DMK12
DMK14
DMP50
DMP53
DMP54
DMP55
VBLKW6
DMP56
DMP58
DLL03
DLL04
VHBLKXl
SMCl
SMC2
SMC3
(TOL)
(BFB)
(DCE)
102 93 100
100 88 99
100 91 103
103 95 105
102 91 99
102 93 106
101 93 104
106 100 111
104' 99 110
105 97 106
102 96 106
111 104 102
109 104 104
98 93 107
100 91 106
104 103 107
100 95 106
96 92 109
92 89 101
99 96 109
87 83 92
102 96 110
110 104 113
104 99 114
100 91 105
95 92 106
Toluene-dB
Bromofluorobenzene
l,2-Dichloroethane-d4
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
--
--
--
--
QC LIMITS
(84-138)
(59-113)
(70-121)
# Column to be used to flag recovery values
* Values outside of contract required QC limits
FORM II VOA-2 OLM03.0
39
I
'9
I
I
I
I
I
I
I ,
I
I
I
•
I
:a
I It
0
B
a. Surrogate Percent Recovery Summary
~ i (Form II SV)
349
I
It
I
I
I
I
I
I
I ,,
I
I
0
2D____ -------
SOIL SEMIVOLATILE SURROGATE RECOVERY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU
Level: (low/med) LOW
Case No. : 25633
Contract: 68D50004
SAS No.: SDG No. : DLL03
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
EPA Sl S2 S3 S4 S5 S6 S7 S8
~f'LE NO. (NBZ) # (FBP)# (TPH)# (PHL) # (2FP) # (TBP) # (2CP) # (DCB)#
------------:;:::;:::;:::;:::;:::;:: ====== ==:::::=== ====== :;:::;::::::::::::;:::;:: :;:::;:::;::;;;:::;:;:: =====:;;; =====:;::;
SBLKRQ 41 38 44 39 40 40 40 36
DMH89 37 37 44 36 34 43 35 31
DMH89MS 46 47 56 46 46 54 46 40
DMH89MSD 49 45 46 46 48 46 48 42
DMH90 40 38 44 39 37 42 38 34
DMH93 50 47 50 48 48 46 49 44
DMH96 38 38 40 38 39 40 39 33 DMJ02 42 42 48 44 42 48 43 36
DMK07 61 60 63 62 67 47 65 54
DMK08 55 53 53 54 57 52 57 48
DMKl0 55 53 54 55 58 52 57 47
DMK12 55 54 56 55 59 51 58 49
DMK14 33 32 44 32 32 42 32 29
DMP50 55 56 . ' 60 56 57 60 57 48
DMP53 36 34 44 36 36 40 36 32
DMP54 41 43 49 44 42 50 43 34
DMH98 51 51 55 48 53 46 52 44
DMJ00 41 44 50 40 40 49 41 37
DMP55 49 49 47 48 50 50 51 43
SBLKRS 26 26* 33 25 21* 26 26 24
DMP55DL 56 55 62 54 51 56 55 47
SBLKRR 56 53 70 53 52 49 54 50
DMP58 48 48 62 47 44 48 46 40
DMP56 66 65 79 68 66 60 70 58
DLL04 31 28* 33 29 28 30 29 26
SBLKAG 46 39 75 42 42 44 42 37
DLL03 66 58 78 68 72 70 72 53
. --
QC LIMITS
Sl (NBZ) Nitrobenzene-d5 (23-120)
S2 (FBP) = 2-Fluorobiphenyl (30-115)
S3 (TPH) Terphenyl-dl4 (18-137)
S4 (PHL) Phenol-d5 (24-113)
S5 (2FP) 2-Fluorophenol (25-121)
S6 (TBP) = 2,4,6-Tribromophenol (19-122)
S7 (2CP) 2-Chlorophenol-d4 (20-130) (advisory)
S8 (DCB) = l,2-Dichlorobenzene-d4 (20-130) (advisory)
# Column to be used to flag recovery values
* Values outside of contract required QC limits
D Surrogate diluted out
--
TOT
OUT
---
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
0
0
1
0
0
--
--
--
page 01 of 01 FORM II SV-2 OLM03.0
350
I
It
I
I
I
I
m
I
I
" u
I
I
I
I
I
: It
I
1,
b. Matrix Spil(e/Nf3.trix Spil(e Duplicate
· Su1111:-;ary
~" (Forn1 III VOA.)
24
I
'9
1
I
I
I
I ,.
I
I
I
0
I
I
3A WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No.: 25633
Matrix Spike -EPA Sample No. : DMK13
SPIKE
ADDED COMPOUND (ug/L) ======================== ---------1,1-Dichloroethene 50.00 Trichloroethene 50.00 Benzene 50.00 Toluene 50.00 Chlorobenzene 50.00
SPIKE
Contract: 68D50004
SAS No.: SDG No. : DLL02
SAMPLE MS MS CONCENTRATION CONCENTRATION % (ug/L) (ug/L) REC # =======:::===== =========:::c:=== ====== 0.000 53.48 107 0.000 49.31 99 0.000 51. 98 104
0.000 49.12 98 0.000 47.26 94
MSD MSD
QC.
LIMITS
REC.
========
61-145
71-120
76-127
76-125
75-130
ADDED CONCENTRATION .. 0 % QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. ==================-===--=--==---= -------------==::::::=== ====== ====== ====== 1,1-Dichloroethene 50.00 56.51 113 5 14 Trichloroethene 50.00 51.02 102 3 14 Benzene 50.00 53.05 106 2 11 Toluene 50.00 50.33 101 3 13 Chlorobenzene 50.00 48.83 98 4 13
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: O out of
Spike Recovery:
COMMENTS:
5 outside limits
0 out of 10 outside limits
FORM III VOA-1
61-145
71-120
76-127
76-125
75,130
OLM03.0
25
I
'-I
I
I
I
I
I
I ,,
I
I
I
• •
m
le
I
n
b. Matrix Spike/Matrix Spike Duplicate
Summary
J: ~· (Form III SV)
287
I
I
I
I
I ,.
I
I
I
I
I
I ,-.
I
I
3C WATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: CompuChem Env. Corp.
Lab Code: COMPU Case No. : 25633
Matrix Spike -EPA Sample No.: DMK13
SPIKE
COM,tofum ADDED
(ug/L) ==========-===-========= ---------Phenol 75.00 2-Chlorophenol 75.00 1,4-Dichlorobenzene 50.00 N-Nitroso-di-n-prop. (1) 50.00 1,2,4-Trichlorobenzene 50.00 4-Chloro-3-methylphenol 75.00 Acenaphthene 50.00 4-Nitrophenol 75.00 2;4-Dinitrotoluene 50.00
Pentachlorophenol 75.00 Pyrene 50.00
SPIKE
Contract: 68D50004
SAS No.: SDG No.: DLL02
SAMPLE MS MS CONCENTRATION CONCENTRATION % (ug/L) (ug/L) REC # --------------------------====== 0.000 55.06 73
0.000 52.30 70 0.000 33.32 67
0.000 34.92 70 0.000 37.28 74
0.000 58.93 78 0.000 43.48 87
0.000 63.30 84 ,.
0.000 40.24 80 0.000 85.96 115* 0.000 54.39 109
MSD MSD
QC.
LIMITS
REC.
=;:;:====
12-110
27-123
36-97
41-116
39-98
23-97
46-118
10-80
24-96
9-103
26-127
ADDED CONCENTRATION % % QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. ---------------------------------=======-===== ====== ::::::::::::::;:::;:::; ====== ====== Phenol 75.00 63.11 84 14 42 2-Chlorophenol 75.00 61.03 81 14 40 1,4-Dichlorobenzene 50.00 38.28 76. 12 28 N-Nitroso-di-n-prop. (1) 50.00 37.26 74 6 38 1,2,4-Trichlorobenzene 50.00 40.34 81 9 28 4-Chloro-3-methylphenol 75.00 63.81 85 8 42 Acenaphthene 50.00 46.10 92 6 31 4-Nitrophenol 75.00 87.51 117* 33 50 2,4-Dinitrotoluene 50.00 44.96 90 12 38 Pentach~orophenol 75.00 99.40 132* 14 -50 Pyrer,,e " 50.00 53. 48 107 2 31
(1) N-Nitroso-di-n-propylamine
# Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits
RPD: 0 out of 11 outside limits Spike Recovery: 4 out of 22 outside limits
COMMENTS:
FORM III SV-1
12-110
27-123
36-97
41-116
39-98
23-97
46-118
10-80
24-96
9-103
26-127
OLM03.0
288
m
It
I
I
I
• g
D
D . ,
I
m
I
I
, I
I
I '-I
I
b. Matrix Spike/Matrix Spil<e Duplicate
· S un1r:1 ary
J: 1. (For1n III V01~-)
24
I
I
I
I
I
3B
SOIL VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: COMPUG-!EM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Matrix Spike -EPA Sample No.: DMP64
SPIKE
ADDED
COMPOUND (ug/Kg)
======================== ---------
1,1-Dichloroethene 65.79
Trichloroethene 65.79
Benzene 65.79
Toluene 65.79
Chlorobenzene 65.79
SPIKE
Contract: 68D50004
SAS No.: SDG No.: DMP60
Level: (low/med) LOW
SAMPLE MS MS CONCENTRATION CONCENTRATION %
(ug/Kg) (ug/Kg) REC #
-------------============= =====::;::
0.000 40.82 62
0.000 44.97 68
0.000 48.01 73
0.000 40.71 62
0.000 40. 46 61
MSD MSD
QC.
LIMITS
REC.
======
59-172
62-137
66-142
59-139
60-133
ADDED CONCENTRATION % % QC LIMITS COMPOUND (ug/Kg) (ug/Kg) REC # RPD # RPD REC. ====================----:;::;::;:::;:;::;:;::::;::;::;: -------------====== ====== ==:::=== ======
1,1-Dichloroethene 65.79 56.74 86 32* 22
Trichloroethene 65.79 74.49 113 50* 24
Benzene 65.79 76.47 116 46* 21
Toluene 65.79 68.92 105 51* 21
Chlorobenzene 65.79 69.46 106 54* 21
# ColuITL~ co be used to flag recovery and RPD values with an asterisk ~ "::
* Values outside of QC limits
RPD: 5 out of
Spike Recovery:
COMM2NTS:
-= -
5 outside limits
O out of 10 outside limits
FORM III VOA-2
59-172
62-137
66-142
59-139
60-133
OLM03.0
25
-1
It
I
I
I
I
I
•
I ,
I
I
I
I
I
I
.It
I
.I
b. Matrix Spike/Matrix Spike Duplicate --
Summary
(Form III SV)
348
I
It
I
I
I
I
I
I
I ,
I
g
B
I
'9
1
I
JD
SOIL SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Matrix Spike -EPA Sample No.: DMP64
SPIKE
ADDED
COMPOUND (ug/Kg)
======================== ---------Phenol 3289
2-Chlorophenol 3289
1,4-Dichlorobenzene 2193
N-Nitroso-di-n-prop. (1) 2193
1,2,4-Trichlorobenzene 2193
4-Chloro-3-methylphenol 3289
Acenaphthene 2193
4-Nitrophenol 3289
2,4-Dinitrotoluene 2193
Pentachlorophenol 3289
Pyrene 2193
SPIKE
Contract: 68D50004
SAS No.: SDG No. : BMl-60
Level: (low/med) LOW
SAMPLE MS MS
CONCENTRATION CONCENTRATION %
(ug/Kg) (ug/Kg) REC #
============= -------------======
0.000 1526 46
0.000 1543 47
0.000 1109 50
0.000 1054 48
0.000 1170 53
0.000 1546 47
0.000 1172 53
0.000 1642
,, .5o -0.000 1211 55
0.000 1126 34
0.000 1177 54
MSD MSD
QC.
LIMITS
REC.
======
26-90
25-102
28-104
41-126
38-107
26-103
31-137
11-114
28-89
17-109
35-142
ADDED CONCENTRATION ,_
0 % QC LIMITS
COMPOUND (ug/Kg) (ug/Kg) REC # RPD # RPD REC. ----------------------------~;-.;=--=====:::::===:;;=== ====== ==:==== ====== =====::;
Phenol 3289 1528 46 0 35
2-Chlorophenol 3289 1536 47 0 50
1,4-Dichlorobenzene 2193 1132 52 4 27
N-Nitroso-di-n-prop. (1) 2193 1059 48 0 38
1,2,4-Trichlorobenzene 2193 1164 53 0 23
4-Chloro-3-methylphenol 3289 1569 48 2 33
Acenaphthene 2193 1174 54 2 19
4-Nitrophenol 3289 1680 51 2 50
2,4-Dinitrotoluene 2193 1280 58 5 47
Pentachlorophenol 3289 711. 4 22 43 47
Pyrene 2193 1324 60 10 36
(1) N-Nitroso-di-n-propylamine
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: 0 out of 11 outside limits
Spike Recovery: O out of 22 outside limits
COMMENTS:
FORM III SV-2
26-90
25-102
28-104
41-126
38-107
26-103
31-137
11-114
28-89
17-109
35-142
OLM03.0
349
~-
It
I
I
I
I
I
I
I ,
I
I
I
I
I
I
It
I
;1
b. Matrix Spil<e/Metrix Spil<e Duplicate
Su11111:.ary
~ ,t (For111 III VOA,)
23
I
I
I
I
I
I ,,
I
I
I
I
I
I
It
I
I
3A
WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No.: 25633
Contract: 68D50004
SAS No.: SDG No.: DMP63
Matrix Spike -EPA Sample No.: DMP79
SPIKE SAMPLE MS MS QC.
ADDED CONCENTRATION CONCENTRATION % LIMITS
COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. -----------------------------------------------------------===::;::== ====== 1,1-Dichloroethene 50.00 0.000 45.31 91 61-145
Trichloroethene 50.00 0.000 43.90 88 71-120
Benzene 50.00 0.000 44.14 88 76-127 Toluene 50.00 0.000 43.73 87 76-125
Chlorobenzene SO.DO 0.000 43.48 87 75-130
SPIKE MSD MSD
ADDED CONCENTRATION % s-0 QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. ======================== ----------------------====== ====== ====== ====== 1,1-Dichloroethene 50.00 46.09 92 1 14 61-145
Trichloroethene 50.00 45.55 91 3 14 71-120 Benzene 50.00 45.76 92 4 11 76-127
Toluene 50.00 45.20 90 3 13 76-125 Chlorobenzene 50.00 44.35 89 2 13 75-130
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: 0 out of
Spike Recovery:
COMMENTS:
5 outside limits
O out of 10 outside limits
FORM III VOA-1 OLM03.0 0,4··. c.. ..
J
It b. Matrix Spike/M-3.trix Spil<e Duplicate
I Sun1r:}ary
I ~ i (Forn1 III V01\)
I ~5033
I c,1/03-;;),~ ()3
. pL----v
I sr:G'
I
I ,.
I
I
I -~ ~
I
1·
I
It --= ·-
I
I 40
I
'-I
I
I
I
I
I
I
fj
I
I
I
I
I
I
It
I
I
3B
SOIL VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPO Case No. : 25633
Matrix Spike -EPA Sample No.: DMH89
SPIKE
ADDED
COMPOUND (ug/Kg)
---------------------------------1,1-Dichloroethene 122.0
Trichloroethene 122.0
Benzene 122.0
Toluene 122.0
Chlorobenzene 122.0
SPIKE
Contract: 68D50004
SAS No.: SDG No.: DLL03
Level: (low/med) LOW
SAMPLE MS MS
CONCENTRATION CONCENTRATION 0 .,
(ug/Kg) (ug/Kg) REC #
============--------------==::===
0.000 114.0 93
0.000 116.1 95
0.000 126.5 104
0.000 121. 0 99
0.000 114.6 94
MSD MSD
QC.
LIMITS
REC.
======
59-172
62-137
66-142
59-139
60-133
ADDED CONCENTRATION %-%-QC LIMITS
COMPOUND (ug/Kg) (ug/Kg) REC # RPD # RPD REC. ----------------------------------------------=====::::: ====== ====== :;:::::;:;:::;::;::;
1,1-Dichloroethene 122.0 123.8 101 8 22
Trichloroethene 122.0 119.6 98 3 24
Benzene 122.0 127.1 104 0 21
Toluene 122.0 123.8 101 2 21
Chlorobenzene 122.0 115.8 95 1 21
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: 0 out of 5 outside limits
Spike Recovery: O out of 10 outside limits
COMMENTS:
FORM III VOA-2
59-172
62-137
66-142
59-139
60-133
OLM03.0
41
I
:'9
I
I
I
·1
:1
I
I ,,
I
I
I
I
I
.1
·~
I
I .I
b. Matrix Spike/Matrix Spike Duplicate
Summary
., i -(Form III SV)
351
I
I
I
I
I
I ,
I
.I
I
I
I
3D
SOIL SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: COMPUCHEM ENV. CORP ..
Lab Code: COMPU Case No. : 2.5,633
Matrix Spike -EPA Sample No.: DMH89
SPIKE ~ i ADDED
COMPOUND (ug/Kg)
======================== ---------
Phenol 6098
2-Chlorophenol 6098
1,4-Dichlorobenzene 4065
N-Nitroso-di-n-prop. (1) 4065
1,2,4-Trichlorobenzene 4065
4-Chloro-3-methylphenol 6098
Acenaphthene 4065
4-Nitrophenol 6098
2,4-Dinitrotoluene 4065
Pentachlorophenol 6098
Pyrene 4065
Contract: 68D50004
SAS No.: SDG No. : DLL03
Level: (low/med) WW
SAMPLE MS MS
CONCENTRATION CONCENTRATION S-0
(ug/Kg) (ug/Kg) REC # --------------------------====== 0.000 2655 44
0.000 2546 42
0.000 1781 44
0.000 1938 48
0.000 1904 47
0.000 3342 55
0.000 2284 56
0.000 3420 56
0.000 2462 60
0.000 2248 37
0.000 2365 58
MSD MSD
QC.
LIMITS
REC.
======
26-90
25-102
28-104
41-126
38-107
26-103
31-137
11-114
28-89
17-109
35-142
SPIKB
ADDED
(ug/Kg)
CONCENTRATION % % QC LIMITS
COMPOUND (ug/Kg) REC # RPD # RPD REC.
====== ::::::::::;::;:;;;:::;; ====== ====== Phenol
2-Chlorophenol
1,4-Dichlorobenzene
N-Nitroso-di-n-prop. (1)
1,2,4-Trichlorobenzene
4-Chloro-3-methylphenol
Acenaphthene
4-Nitrophenol
2,4-Dinitrotoluene
Pentachkirophenol
Pyrerre ~
(1) N-Nitroso-di-n-propylamine
6077
6077
4052
4052
4052
6077
4052
6077
4052
6077
4052
2683
2676
1916
2020
1994
2895
2026
3172
2179
1636
2023
44
44
47
50
49
48
50
52
54
27
50
0 35
5 50
6 27
4 38
4 23
14 33
11 19
7 50
10 47
31 · -4 7
15 36
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: O out of 11 outside limits
Spike Recovery: O out of 22 Ol\,~side limits
COMf'/JENTS :
FORM III SV-2
26-90
25-102
28-104
41-126
38-107
26-103
31-137
11-114
28-89
17-109
35-142
OLM03.0
352
11
• I
c. Method Bla11k: Si1111111ary (F or111 IV VOA)
I ~%
If n1ore than a single fonn is necessary, forn1s shall
be arranged in chro;~ological order by date of
analysis of the blanks and by instru111ent. I
I
I
'I
I
I
I
·1
\I
I
It
I
~ -
-~-4c.
--.::...
26
'
I
I
I
I
'
I
I
I
I
I
I
4A EPA SAMPLE NO. VOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: CB970818C55
Date Analyzed: 08/18/97
GC ColV: DB624
Instrument ID: F50055
ID: 0. 53 (mm)
Contract: 68D50004
SAS No.:
VBLKMM
SDG No. : DLL02
Lab Sample ID: VBLKMM
Time Analyzed: 0659
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
2.2
~· ~3
COMMENTS:
24
25
26
27
28
29
30
EPA LAB
SAMPLE NO. SAMPLE ID
=:::::.=====--=== --------------DMH91 864726
DMH92 864733
DMH94 864 734
LAB TIME
FILE ID ANALYZED
=====:;:.=---==------------CN064'726A55 1241
CN064733A55 1321
CN064 734A55 1400
. -
e
lt=,age 01 .Qj: 91
FORM IV VOA OLM03.0 I
I
27
I
~
I
I
I
I
I
I
I ,
I
I
11
I
I
:1
4A EPA SAMPLE NO. VOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV.
Lab Code: COMPU Case
Lab File ID: CB970821B55
Date Analyzed: 08/21/97
GC Col~:-DB624 ID:
Instrument ID: F50055
CORP.
No.: 25633 ..
0.53 ( mm)
Contract: 68D50004
SAS No.:
VBLKTG
SDG No. : DLL02
Lab Sample ID: VBLKTG
Time Analyzed: 2044
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
;;.2
~ "'23
24
25
26
27
28
29
30
COMMENTS:
EPA
SAMPLE NO.
=====:::::=---==
DMH95
DMH97
DMH99
DMJ0l
DMK06
LAB
SAMPLE ID
--------------
864735
864736
864738
864 739
864740
LAB TIME
FILE ID ANALYZED
===::;:===--===== ==========
CN064735B55 0426
CN064736B55 0505
CN064738B55 0544
CN064739B55 0623
CN064740B55 0703
.
. -
'
·1e:,age 01 gJ _01
FORM IV VOA OLM03.0
B
,I
28
4A EPA SAMPLE NO.
I
I
I
I
I
I ,
I
I
I
I
I
VOLATILE METIIOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: CB970822A55
Date Analyzed: 08/22/97
GC Coll~' DB624
Instrument ID: F50055
ID: 0.53 (mm)
Contract: 68D50004
SAS No.:
VBLKXG
SDG No. : DLL02
Lab Sample ID: VBLKXG
Time Analyzed: 0856
Heated Purge: (Y/N) N
THIS METIIOD BLANK APPLIES TO TI-IE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22 .,_. "2 3
COMMENTS:
24
25
26
27
28
29
30
01 of 01 --
EPA
SAMPLE NO.
=======-===::;
DMK09
DMKll
DMK13
DMP51
DMP52
DMP57
DMP59
DMP61
DMK13MS
DMK13MSD
LAB
SAMPLE ID
===--==;:---==-
864741
864 742
864743
864744
864 745
864 746
864747
864748
864727
864728
LAB TIME
FILE ID ANALYZED
=======--==::::-= ======--== CN064741A55 1024
CN064742A55 1113
CN064743A55 1146
CN064744A55 1220
CN064745A55 1255
CN064746A55 1336
CN064747A55 1416
CN064748A55 1451
CN064727A55 1741
CN064728A55 1825
. -
I
~age
I
FORM IV VOA OLM03.0
29
.I
I
I
I
I
I
I ,
I
I
I
I
I
I
4A
VOLATILE METHOD BLANK SUMMARY EPA SAMPLE NO.
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: CB970823A55
Date Analyzed: 08/23/97
GC Col~: DB624
Instrument ID: F50055
ID: 0.53 (mm)
Contract: 68050004
SAS No.:
VBLKYY
SDG No. : DLL02
Lab Sample ID: VBLKYY
Time Analyzed: 0704
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
'22
~ °"23
24
25
26
27
28
29
30
COMMENTS:
EPA
SAMPLE NO.
------------
DLL02
DLL05
DLL06
LAB
SAMPLE ID
--------------
864761
864762
864763
LAB TIME
FILE ID ANALYZED
============== ::;::;::;:::;::;::;;::;::::;::;
CR064761A55 0840
CR064762A55 0918
CR064763A55 0956
--
It page 01....Qf _01
I
I
FORM IV VOA OLM03.0
30
-
" I
I
I
I
I
I
I ,
I
I
I
_I
••
I
4A EPA SAMPLE NO. VOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No.: 25633
Lab File ID: CB970902A55
Date Analyzed: 09/02/97
GC Column: DB624 .J,_ i.
Instrument ID: F50055
ID: 0.53 (mm)
Contract: 68D50004
SAS No.:
VBLKQA
SDG No. : DLL02
Lab Sample ID: VBLKQA
Time Analyzed: 0841
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
2.2
~-'23
24
25
26
27
28
29
30
COMMENTS:
EPA
SAMPLE NO.
============
VHBLKG7
LAB
SAMPLE ID
==;;;;==::========
864730
.
LAB TIME FILE ID ANALYZED
============== ----------CN064730A55 1059
'
--
I ~age
I
01 of 01
FORM IV VOA OLM03.0
31
I
••
'-I
I
I
I
I
I
I ,
I
I
I
I
I
I
It
I
I
c. Method Blank Summary (Form IV SV)
V .tmore than a single · form is necessary, forms shall be
arranged in chronological order by date of analysis and by
instrument.
289
I
I
I
I
I
:1
4B EPA SAMPLE NO. SEMIVOLATILE METHOD BLANK SUMMARY
Lab Name: CompuChem Env. Corp.
1-:..:..
Lab Code< COMPU Case No. : 25633
Lab File ID: GH065194A60
Instrument ID: 5972HP60
Matri~~ Jspiliwater) WATER
Level: (low/med) LOW
Contract: 68D50004
SAS No.:
SBLKTG
SDG No. : DLL02
Lab Sample ID: 865194
Date Extracted: 08/18/97
Date Analyzed: 08/24/97
Time Analyzed: 0910
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
~ :12 23
24
25
26
27
28
29
30
COMMENTS:
01 of 61
EPA
SAMPLE NO.
------------
DMH91
DMH95
DMH97
DMH99
DMJ0l
DMK06
DMK09
DMH92
DMKll
DLL05
DLL06
DLL02
DMH94
LAB
SAMPLE ID
-===::::=========
864726
864735
864 736
864 738
864739
864740
864 741
864 733
864 742
864762
864763
864 761
864 734
LAB DATE
FILE ID ANALYZED
=========::::::::::::;::;::::: ----------GH064726A60 08/24/97
GH064735A60 08/24/97
GH064736A60 08/24/97
GH064738A60 08/24/97
GH064739A60 08/24/97
GH064740A60 08/24/97
GH064741A60 08/24/97
GH064733A60 08/24/97
GH064742B60 08/24/97
GH064762B60 08/24/97
GH064763B60 08/24/97
GH064761B60 08/25/97
GJ064 734A60 08/25/97
. -
FORM IV SV-1 OLM03.0
290
4B EPA SAMPLE NO. -,
..
I
I
I
I
I
I
I ,
I
I
I
I
I
SEMIVOLATILE METHOD BLANK SUMMARY
Lab Name: CompuChem Env. Corp.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH065196A60
Instrument ID: 5972HP60
Matrix~ /;soil/water) WATER
Level: (low/med) LOW
Contract: 68DS0004
SAS No.:
SBLKTH
SDG No. : DLL02
Lab Sample ID: 865196
Date Extracted: 08/19/97
Date Analyzed: 08/25/97
Time Analyzed: 1827
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
:--~ 23
24
25
26
27
28
29
30
COMMENTS:
01 at 01
EPA
SAMPLE NO.
------------
DMK13
DMK13MS
DMK13MSD
DMP52
DMP57
DMPSl
DMP61
DMP59
LAB
SAMPLE ID
-----=--==-===
864743
864731
864732
864 745
864 746
864744
864 748
864 74 7
LAB DATE
FILE ID ANALYZED
=::=:=--==--==----===-===-=
GH064743A60 08/25/97
GH064731A60 08/25/97
GH064732A60 08/25/97
GH06474SA60 08/25/97
GH064746A60 08/25/97
GH064744A60 08/26/97
GH064748C60 08/26/97
GH064747C60 08/26/97
. -
I
laage
I FORM IV SV-1 OLM03.0
291 I
I
-I
I
I
I
I
I
I ,
I
I
I
I
I
I
-'9
I
I I
c. Metl1od Blanl< S1~1n111ary (For111 IV VOA)
If 111ore than a single form is necessary, forn1s shall
be arranged in clu-cnological order by date of
analysis cif the.black~: and by instrun1ent.
26
4A EPA SAMPLE NO.
I
'9
1
I
I
I
I
I
I ,,
I
I
I
I
D
VOLATILE METilOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH064803B51
Date Analyzed: 08/20/97
GC ColuJU7,r·DB624
Instrument ID: F50051
ID: 0 . 53 ( mm)
Contract: 68D50004
SAS No.:
VBLKX3
SDG No. : DMP60
Lab Sample ID: 864803
Time Analyzed: 2245
Heated Purge: (Y/N) Y
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
:Z-2 .-23
COMMENTS:
24
25
26
27
28
29
30
01 ..o-£ .01
EPA
SAMPLE NO.
------------
DMP64
DMP70
DMP71
DMP72
DMP74
DMP75
DMP64MS
LAB
SAMPLE ID
--------------864704
864 714
864715
864 716
864718
864719
864705
LAB TIME
FILE ID ANALYZED
----------------====----
GH064704B51 2344
GH064714B51 0217
GH064715B51 0254
GH064716B51 0330
GH064718B51 0442
GI-i064719B51 0518
GH064705B51 0554
-
. -
I
~age
I FORM IV VOA OLM03.0
27
4A EPA SAMPLE NO.
I -.
I
I
I
I
I
I
I ,,
I
VOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH065763A52
Date Analyzed: 08/21/97
GC Col~i · DB624
Instrument ID: F50052
ID: 0.53 (mm)
Contract: 68D50004
SAS No.:
VBLKYl
SDG No. : DMP60
Lab Sample ID: 865763
Time Analyzed: 0756
Heated Purge: (Y/N) Y
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
2-2 ~ ~3
COMMENTS:
24
25
26
27
28
29
30
01 .cl .01
EPA
SAMPLE NO.
============
DMP65
DMP66
DMP67
DMP73
DMP64MSD
LAB
SAMPLE ID
--------------
864711
864712
864 713
864717
864706
LAB TIME
FILE ID ANALYZED
--------------=:::::========
GR064711A52 112'3
GR064712A52 1211
GR064713A52 1322
GR064717A52 1359
GR064706A52 1433
. -
I
,.age
I FORM IV VOA OL.NJ03. 0
I 28
I
-I
I
I
I
I
I
I ,
I
I
I
I
I
I
4A EPA SAMPLE NO.
VOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH064795B52
Date Analyzed: 08/21/97
GC Col~i DB624
Instrument ID: F50052
ID: O. 53 (mm)
Contract: 68D50004
SAS No.:
VBLKW6
SDG No. : DMP60
Lab Sample ID: 864795
Time Analyzed: 1853
Heated Purge: (Y/N) Y
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
~ "2.2 23
24
25
26
27
28
29
30
COMMENTS:
EPA
SAMPLE NO.
------------
DMP60
DMP62
DMP77
DMP78
DMP81
LAB
SAMPLE ID
--------------
864 702
864 703
864721
864722
864723
LAB TIME
FILE ID ANALYZED
------------------------
'GH064 702B52 2157
GH064703B52 2239
GH064721B52 2359
GH064722B52 0045
GH064723B52 0123
. -
'
ltpage
I
0l~f-01
FORM IV VOA OL.IVJ03. 0
I 29
I
I
I
I
I ,
I
I
I
I
I
I
4A EPA SAMPLE NO.
VOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH065474B52
Date Analyzed: 08/22/97
GC Col1¾"1i DB624
Instrument ID: F50052
ID: 0.53 (mm)
Contract: 68D50004
SAS No.:
VBLKDl
SDG No.: DMP60
Lab Sample ID: 865474
Time Analyzed: 1907
Heated Purge: (Y/N) Y
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
EPA LAB LAB TIME
SAMPLE NO. SAMPLE ID FILE ID ANALYZED
------------;::;===----=====-============== ========== 01 DMP76 864720 G2R64720B52 2052
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21 .
:n -
" 23
24
25
26
27
28
29 .
30
I
COMMENTS:
~age
I
01 ..cf ..ill
FORM IV VOA OLM03.0
I 30
:I
-I
I
I
I
I
I
I ,
I
I
I
I
I
I
4A EPA SAMPLE NO.
VOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH066220B52
Date Analyzed: 08/24/97
GC Col~ DB624
Instrument ID: F50052
ID: o. 53 (mm)
Contract: 6BD50004
SAS No.:
VBLKLl
SDG No.: DMP60
Lab Sample ID: 866220
Time Analyzed: 2010
Heated Purge: (Y/N) Y
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
EPA LAB LAB TIME
SAMPLE NO. SAMPLE ID FILE ID ANALYZED
------------=------:::; _____ ::::; ------------------==----01 VHBLKX3 864707 GH064707B52 0306
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
2-2 -~ "23
24
25
26
27
28
29
30
COMMENTS:
lltpage
I
01 _of _01
FORM IV VOA OLM03.0
I 31
-1
'9 c. Method Blank Summary (Form IV SV)
I
If more than a single form is necessary, forms shall be I arranged in chronological order by date of analysis and by
I
I
I
I
I ,
I
I
I
I
I
I
It
I
I
instrument
350
_I
---1
I
I
I
I
I
I ,
I
I
I
I
I
I
4B EPA SAMPLE NO.
SEMIVOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV, CORP,
Lab Code: COMPU Case No. : 25633
Lab File ID: GJ064768A66
Instrument ID: 5972HP66
Matrix: (soil/water) SOIL
Level: (low/med) LOW
Contract: 68D50004
SAS No.:
SBLKRS
SDG No , : 13MP6{)
Lab Sample ID: 864768
Date Extracted: 08/15/97
Date Analyzed: 09/17/97
Time Analyzed: 1428
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD
COMMENTS:
-Ol_
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
EPA
SAMPLE NO.
------------
DMP64
DMP64MS
DMP64MSD
DMP65
DMP72
DMP65RE
DMP67
DMP70
DMP75
DMP76
DMP77
DMP78
DMP76DL
LAB
SAMPLE ID
--------------864 704''
864709
864710
864711
864 716
864 711
864713
864 714
864719
864720
864721
864 722
864720
••
LAB DATE
FILE ID ANALYZED
' ------------------------
GH064704A66 09/17/97
GH064709A66 09/17/97
GH064710A66 09/17/97
GH064711A66 09/17/97
GH064716A66 09/17/97
GJ064711A66 09/18/97
GJ064713A66 09/18/97
GH064714A66 09/18/97
GH064719A66 09/18/97
GH064720A66 09/18/97
GH064721A66 09/18/97
GH064722A66 09/18/97
GD064720A66 09/19/97
I.page 01 of 01
FORM IV SV-1 OLM03.0
I
••
351
-----=
I
I
I
I
I -.,
I
I
I
I
I
I
4B EPA SAMPLE NO.
SEMIVOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GJ064766A66
Instrument ID: 5972HP66
Matrix: (soil/water} SOIL ••
Level: (low/med} WW
Contract: 68D50004
SAS No.:
SBLKRR
SDG No . : BMPti-0
Lab Sample ID: 864766
Date Extracted: 08/15/97
Date Analyzed: 09/18/97
Time Analyzed: 1117
THIS METHOD BLANK APPLIES TO THE FOLWWING SAMPLES, MS and MSD
COMMENTS:
Ol
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
EPA
SAMPLE NO.
------------
DMP60
DMP62
LAB
SAMPLE ID
--------------
864702
864703
LAB DATE
FILE ID ANALYZED
------------------------
GJ064702A66 09/18/97
GJ064 703A66 09/18/97
'9 page 01 of 01
FORM IV SV-1 OL.1\103. 0
I
-1
352
I
I
I
I
I
I ,
I
I
I
I
I
I
4B EPA SAMPLE NO.
SEMIVOLATILE METiiDD BLANK SUMMARY
Lab Name: COMPUCTIEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH068696A66
Instrument ID: 5972HP66
Matrix: (soil/water) SOIL
Level: (low/med) LOW
SBLKZV
Contract: 68D50004
SAS No . : SDG No . : BMP&O
Lab Sample ID: 868696
Date Extracted: 09/18/97
Date Analyzed: 09/20/97
Time Analyzed: 1226
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD
COMMENTS:
. 01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
.26
27
28
29
30
EPA
SAMPLE NO.
=====:::======
DMP66
DMP73
DMP74
LAB
SAMPLE ID
--------------
864712
864717
864 718' •
LAB. DATE
FILE ID ANALYZED
' =======-====== ----------
GR064712A66 09/20/97
GR064717A66 09/20/97
GR064718A66 09/20/97
"lltpage 01 of 01
FORM IV SV-1 OLM03.0
m
.I
353
I
I
I
I
I
I
I ,
I
I
I
I
I
4B EPA SAMPLE NO.
SEMIVOLATILE METIJOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH069009A66
Instrument ID: 5972HP66
Matrix: (soil/water) SOIL
Level: (low/med) WW
Contract: 68D50004
SAS No.:
SBLKAG
SDG No . : IlMPtrO
Lab Sample ID: 869009
Date Extracted: 09/19/97
Date Analyzed: 09/22/97
Time Analyzed: 0954
TIJIS METIJOD BLANK APPLIES TO THE FOLWWING SAMPLES, MS and MSD
OL
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
EPA
SAMPLE NO.
------------
DMP71
LAB
SAMPLE ID
--------------
864715
.• -
LAB DATE
FILE ID ANALYZED ' --------------======---~
GR064715A66 09/22/97
.
COMMENTS: i•
~age 01 of 01
·PORM IV SV-1 OLM03.0
I 354
.1
It
I
I
I
I
I
I
I ,.
I
I
I
11
I
I
It
I
(0
c. Method Bla11l( Stn1111ary (For111 IV VOA)
' If 111ore than a sing!e forn1 is necessary, forn1s shall
. be arranged in chronological order by date of
analysis of the blanL:: and by instrun1ent.
25
I
I
I
I
I
I ,
I
I
I
I
I
I
'-
4A EPA SAMPLE NO.
VOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: CB970822B55
Date Analyzed: 08/22/97
GC Colurfu ~ DB624
Instrument ID: F50055
ID: 0. 53 (mm)
Contract: 68D50004
SAS No.:
VBLKTA
SDG No. : DMP63
Lab Sample ID: VBLKTA
Time Analyzed: 2054
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
2_0
~ .ll
22
23
24
25
26
27
28
29
30
COMMENTS:
--. ·-
EPA
SAMPLE NO.
------------
DMP80
LAB LAB TIME
SAMPLE ID FILE ID ANALYZED
--------------------------------------864757 CN064757B55 2309
I page 01 of 01
FORM IV VOA OLM03.0
I 26
I
I
I
I
I
I
I
I
I
I
I
It
4A EPA SAMPLE NO.
VOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No.: 25633
Lab File ID: CB970824B55
Date Analyzed: 08/25/97
GC Colu1tn ~ DB624
Instrument ID: F50055
ID: 0. 53 (mm)
Contract: 68D50004
SAS No.:
VBLKTJ
SDG No. : DMP63
Lab Sample ID: VBLKTJ
Time Analyzed: 0131
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
~ ,21
22
23
24
25
26
27
28
29
30
COMMENTS:
EPA
SAMPLE NO.
------------
VHBLKV5
LAB
SAMPLE ID
--------------
864756
LAB TIME
FILE ID ANALYZED
------------------------CN064756B55 0327
m page 01 of 01
FORM IV VOA OLM03.0
27 ..
I
I
I
I
I
I
I
1I
' I
I
I
4A EPA SAMPLE NO.
VOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No.: 25633
Lab File ID: CB970822A55
Date Analyzed: 08/22/97
GC Coliffnn~ DB624 ID: 0.53 (mm)
Instrument ID: F50055
Contract: 68D50004
SAS No.:
VBLKXG
SDG No. : DMP63
Lab Sample ID: VBLKXG
Time Analyzed: 0856
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
~ ~l
22
23
24
25
26
27
28
29
30
EPA
SAMPLE NO.
------------
DMP63
DMP68
DMP69
LAB
SAMPLE ID
--------------
864749
864750
864 751
LAB TIME
FILE ID ANALYZED
=====;;;::;;::;;:::::::::==== ==========
CN064749A55 1525
CN064750A55 1603
CN064751A55 1644
I COMMENTS:
''9 ,1 page 01 of 01
FORM IV VOA OLM03.0
28
I
I
I
I
I
I ,
I
I
I
I
I
I
It
4A EPA SAMPLE NO.
VOLATILE METIIOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPO Case No. : 25633
Lab File ID: CB970823A55
Date Analyzed: 08/23/97
GC Coli:lfui~ DB624 ID: 0. 53 (mm)
Instrument ID: F50055
Contract: 68D50004
SAS No.:
VBLKYY
SDG No. : DMP63
Lab Sample ID: VBLKYY
Time Analyzed: 0704
Heated Purge: (Y/N) N
_TIIIS METIIOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and_MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
-· _J1 22
COMMENTS:
23
24
25
26
27
28
29
30
EPA
SAMPLE NO.
------------
DMP79
DMP79MS
DMP79MSD
DMP98
LAB
SAMPLE ID
==============
864752
864753
864 754
864758
LAB TIME
FILE ID ANALYZED
------------------------CR064752A55 0752
CR064753A55 1359
CR064 754A55 1526
CR064758A55 1605
I page 01 of 01
FORM IV VOA OLM03.0
29
:1
It
I
I
I
I
I
I
I ,
I
I
I
I
I
I
It
ii
I
c. Method Blank: Suan1nary (For1n IV VOA)
~ I If 111ore than a single forn1 is necessary, fonns shall
be arranged in chronological order by date of
analysis of the blarJ:~; and by instru1nent.
42
.I
lit
I
I
I
I
I
I
I ,,
n
I
I
I
I
I
It
4A EPA SAMPLE NO.
VOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH064783A52
Date Analyzed: 08/19/97
GC Colu~~ DB624
Instrument ID: F50052
ID: 0.53 (mm)
Contract: 68D50004
SAS No.:
VBLKV9
SDG No.: DLL03
Lab Sample ID: 864783
Time Analyzed: 1356
Heated Purge: (Y/N) Y
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
" '21
22
23
24
25
26
27
28
29
30
COMMENTS:
EPA
SAMPLE NO.
------------
DMH89
DMH90
DMH93
DMH96
DMH98
DMJ00
DMJ02
DMK07
DMK08
DMKl0
DMH89MS
DMH89MSD
LAB
SAMPLE ID
--------------
864678
864685
864686
864687
864688
864689
864690
864691
864692
864693
864679
864680
LAB TIME
FILE ID ANALYZED
============== ;::;;:::::;;;:;;;;;::::::::;::::::::::
GH064678A52 1454
GH064685A52 1535
GH064686A52 1610
GH064687A52 1648
GH064688A52 1725
GH064689A52 .1834
GH064690A52 1911
GH064691A52 1954
GH064692A52 2031
GH064693A52 2108
GH064679A52 2143
GH064680A52 2221
; I page 01 of 01
FORM IV VOA OLM03.0
43
I
.It
I
I
I
I
I
I
I ,
I
I
I
I
I
I
It
4A EPA SAMPLE NO.
VOLATILE METI-IOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH064793A52
Date Analyzed: 08/20/97
GC Colu~; DB624
Instrument ID: F50052
ID: 0. 53 (mm)
Contract: 68D50004
SAS No.:
VBLKW5
SDG No.: DLL03
Lab Sample ID: 864793
Time Analyzed: 1304
Heated Purge: (Y/N) Y
THIS METI-IOD BLANK APPLIES TO TI-IE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
2_9
,,, i1
22
23
24
25
26
27
28
29
30
COMMENTS:
EPA
SAMPLE NO.
------------DMK12
DMK14
DMP50
DMP53
DMP54
DMP55
LAB
SAMPLE ID
--------------864694
864695
864696
864697
864698
864699
LAB TIME
FILE ID ANALYZED
------------------------GH064694B52 1537
GH064695B52 1623
GH064696B52 1702
GH064697B52 1742
GH064698B52 1818
GH064699B52 1858
I page 01 of 01
FORM IV VOA OLM03.0
~-44
I
I
I
I
I ,
I
I
I
I
I
I
'9
4A EPA SAMPLE NO.
VOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH064795B52
Date Analyzed: 08/21/97
GC Collltm~ DB624 ID: 0.53 (mm)
Instrument ID: F50052
Contract: 68D50004
SAS No.:
VBLKW6
SDG No. : DLL03
Lab Sample ID: 864795
Time Analyzed: 1853
Heated Purge: (Y/N) Y
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
!" ,t1
22
23
24
25
26
27
28
29
30
COMMENTS:
EPA
SAMPLE NO.
---====----=
DMP56
DMP58
DLL03
DLL04
VHBLKXl
LAB
SAMPLE ID
:::::=============
864700
864701
864724
864 725
864681
LAB TIME
FILE ID ANALYZED
=======:==== '== ==========
GH064700B52 2036
GH064701B52 2120
GH064724B52 0201
GH064725B52 0249
GH064681B52 0326
1 page 01 of 01
FORM IV VOA OLM03.0
.I 45
I
--I
I
I
I
I
I
I !,
I
I
I
I
I
I
-It
I
-~1
c. Method Blank Summary (Form IV SV)
~If more than a single form is necessary, forms shall be
arranged in chronological order by date of analysis and by
instrument.
353
I
'-I
4B EPA SAMPLE NO.
I
I
I
I
I
I ,
I
I
I
SEMIVOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH069009A66
Instniment ID: 5972HP66
Matrix:~(~oil/water) SOIL
Level: (low/med) LOW
Contract: 68D50004
SAS No.:
SBLKAG
SDG No. : DLL03
Lab Sample ID: 869009
Date Extracted: 09/19/97
Date Analyzed: 09/22/97
Time Analyzed: 0954
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
2-1
,; ~2
COMMENTS:
23
24
25
26
27
28
29
30
01 of 01
EPA
SAMPLE NO.
============
DLL03
• LAB
SAMPLE ID
--------------
864 724
..
LAB DATE
FILE ID ANALYZED
----------,--------------GR064724A66 09/22/97
-
I
~page
I FORM IV SV-1 OLM03.0
I 354
I
It
I
4B EPA SAMPLE NO.
I
I
I
I
I
I
~
I
I
I
I
I
SEMIVOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH064764A66
Instrument ID: 5972HP66
Matrix:i(!oil/water) SOIL
Level: (low/med) LOW
...
Contract: 68D50004
SAS No.:
SBLKRQ
SDG No. : DLL03
Lab Sample ID: 864764
Date Extracted: 08/15/97
Date Analyzed: 09/16/97
Time Analyzed: 1312
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
2-1
-· '£2
23
24
25
26
27
28
29
30
COMJViENTS:
--01 of 01
EPA
SAMPLE NO.
------------
DMH89
DMH89MS
DMH89MSD
DMH90
DMH93
DMH96
DMJ02
DMK07
DMK08
DMKl0
DMK12
DMK14
DMP50
DMP53
DMP54
DMH98
DMJ00
DMP55
DMP55DL
LAB
SAMPLE ID
---, ----------
864678
864683
864684
864685
864686
864687
864690
864691
864692
864693,,
864694
864695
864696
864697
864698
864688
864689
864699
864699
LAB DATE
FILE ID ANALYZED
------------------------GH064678A66 09/16/97
GH064683A66 09/16/97
GH064684A66 09/16/97
GH064685A66 09/16/97
GH064686A66 09/16/97
GH064687C66 09/17/97
GH064690C66 09/17/97
GH064691C66 09/17/97
GH064692C66 09/17/97
GH064693C66 09/17/97
GH064694C66 09/17/97
GH064695C66 09/17/97
GH064696C66 09/17/97
GH064697C66 09/17/97
GH064698C66 09/17/97
GH064688C66 09/17/97
GH064689C66 09/17/97
GH064699C66 09/17/97
GD064699A66 09/17/97
.
. -
I
'I.page
I FORM IV SV-1 OLM03.0
355
I
It
I
I
I
I
I
I
I ,
I
0
m
I
I
I
4B EPA SAMPLE NO.
SEMIVOLATILE METIJOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GJ064766A66
Instrument ID: 5972HP66
Matrix:.):(~oil/water) SOIL
Level: (low/med) LOW
Contract: 68D50004
SAS No.:
SBLKRR
SDG No. : DLL03
Lab Sample ID: 864766
Date Extracted: 08/15/97
Date Analyzed: 09/18/97
Time Analyzed: 1117
TilIS METilOD BLANK APPLIES TO TIJE FOLLOWING.SAMPLES, MS and MSD
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
2J.
~ ~2
23
24
25
26
27
28
29
30
COMMENTS:
EPA
SAMPLE NO.
------------DMP58
DMP56
LAB
SAMPLE ID . , ==============
864701
864700
.
.. ,
'
LAB DATE
FILE ID ANALYZED
:;::::;::;;;::::::::======== ----------GJ064701A66 09/18/97
GJ064700A66 09/18/97
-
l,page
I
--01 of 01
FORM IV SV-1 OLM03.0
--356
I
It
I
I
I
I
I
I
I ,
I
I
I
4B EPA SAMPLE NO.
SEMIVOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GJ064768A66
Instrument ID: 5972HP66
Matrix:J-(Eoil/water) SOIL
Level: (low/med) LOW ••
Contract: 68D50004
SAS No.:
SBLKRS
SDG No. : DLL03
Lab Sample ID: 864768
Date Extracted: 08/15/97
Date Analyzed: 09/17/97
Time Analyzed: 1428
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20 :u
., £2
23
24
25
26
27
28
29
30
COMMENTS:
EPA
SAMPLE NO.
------------DLL04
LAB
SAMPLE ID
--------------
864725
.
LAB DATE
FILE ID ANALYZED
--------------==========
GJ064725A66 09/19/97
. ..
'-page
I
01 or Lil
'flORM IV SV-1 OLM03.0
I 357
U.S. EPA -CLP
SA
EPA SAMPLE NO.
SPIKE SAMPLE RECOVERY
rab Name: CHEMTECH CONSULTING
~ab Code: CHEM Case No.:
·tatrix (soil/water): SOIL
% Solids for Sample: 36.8
GROUP
25633
MDLL03S
Contract: 68-DS-0166
SAS No.: SDG No.: MDMP99
Level (low/med): LOW
I Concentration Units (ug/L or mg/kg dry weight): MG/KG
Control " • Limit Spiked Sample Sample Spike
Analyte %R· Result (SSR) C Result (SR) C Added (SA) %R Q
J\.luminum
I Antimony 75-125 204.0503 3.2133 B 198.35 101.3
Arsenic 75-125 21.0013 5.1214 15.87 100.1
Barium 75-125 1023.5401 228.9987 793.40 100.1
I Beryllium 75-125 24.4684 2.6103 19.83 110.2
Cadmium 75-125 20.8347 0.3967 u 19.83 105.1
Calcium
romium 75-125 146.8264 62.9324 79.34 105.7
balt 75-125 224.5636 22.1914 198.35 102.0
75-125 150.4998 41.5424 99.17 109.9
55.1690 46.4773 7.93 109.6
Magnesium
Manganese 75-125 833.8345 627.3802 198.35 104.1
Mercury 75-125 1.2582 0.2717 u 1.36 92.5
Nickel 75-125 229.5977 27.4199 198.35 101.9
Potassium
Selenium 75-125 6.6050 2.8205 3.97 95.3
Silver 75-125 21.3662 0.7934 u 19.83 107.7
75-125 23.6790 3.0308 B 19.83 104.1
Vanadium 75-125 318 .4148 105.0222 198.35 107.6
75-125 347.0803 133.2037 198.35 107.8
lomments:
!
I
It
I FORM V (Part 1) -IN 000036 ILM04.0
I
M
NR
p
p
p
p
p
NR
p
p
p
NR
p
NR
p
CV
p
NR
p
p
NR
p
p
p
NR
I U.S. EPA -CLP
SA
EPA SAMPLE NO. It SPIKE SAMPLE RECOVERY
MDMK13S lab Name: CHEMTECH CONSULTING Contract: 68-DS-0166
Lab Code: CHEM Case No.:
GROUP
25633 SAS No. : SDG No. : MDMP98
latrix (soil/water): WATER Level (low/med): LOW
% Solids for Sample: 0.0
I Concentration Units (ug/L or mg/kg dry weight): UG/L
Control " • Limit Spiked Sample Sample Spike -~ AnalyCe %R. Result (SSR) C -Result (SR) C Added (SA) %R Q
Aluminum ---75-125 1991.7000 180.8400 B 2000.00 90.5 I Antimony 75-125 483.5200 5.0000 u 500.00 96.7
Arsenic 75-125 44.9800 7.0000 u 40.00 112.4
Barium 75-125 1902.6900 24.2600 B 2000.00 93.9
I Beryllium 75-125 53.3200 1.0000 u 50.00 106.6
Cadmium 75-125 48.6800 1.0000 u 50.00 97.4
Calcium
romium 75-125 198.2500 3.0400 .B 200.00 97.6
alt 75-125 485.2200 2.0000 u 500.00 97.0
Copper 75-125 243.6400 2.4200 B 250.00 96.5
Iron 75-125 2335.9400 1306.0000 1000.00 103.0
I Lead 75-125 18.7800 2.0000 u 20.00 93. 9
Magnesium
Manganese 75-125 835.9600 347.1800 500.00 97.8
Mercury 75-125 0.8610 0.2000 u 1.00 86.1
!ickel 75-125 488.9900 2.8600 B 500.00 97.2
otassium
elenium 75-125 11.7600 5.0000 u 10.00 117.6
'ilver 75-125 52.2600 2.0000 u 50.00 104.5
odium
Thallium 75-125 54.4400 6.0000 u 50.00 108.9
'"'nadium 75-125 493.3800 1.0800 B 500.00 98.5
inc 75-125 497.7600 5.9200 B 500.00 98.4
yanide
lmments:
---
FORM V (Part 1) -IN 000047 ILM04.0
D
M
-p
p
p
p
p
p
NR
p
p
p
p
p
NR
p
CV
p
NR
p
p
NR
p
p
p
NR
-
I
U.S. EPA -CLP
5A I
It
EPA SAMPLE NO.
SPIKE SAMPLE RECOVERY
!tab Name: CHEMTECH CONSULTING
'lab Code: CHEM Case No.:
tatrix (soil/water): WATER
% Solids for.Sample: 0.0
GROUP
25633
MDMP63S
Contract: 68-D5-0166
SAS No.: SDG No.: MDMP63
Level (low/med): LOW
I Concentration Units (ug/L or mg/kg dry weight): UG/L
Control ,, • Liffi-i-t Spiked Sample Sample Spike
Analyte %R. Result (SSR) C Result (SR) C Added (SA) %R Q
75-125 1913.1300 55.5900 B 2000.00 92.9
75-125 496.8200 5.0000 u 500.00 99.4
75-125 42.0200 7.0000 u 40.00 105.0
Barium 75-125 1957.8800 29.7200 B 2000.00 96.4
Beryllium 75-125 53.8100 1.0000 u 50.00 107.6
Cadmium 75-125 49.8900 1.0000 u 50.00 99.8
Calcium
romium 75-125 194.0200 1.0000 u 200.00 97.0
balt 75-125 491.2200 2.0000 u 500.00 98.2
75-125 250.4200 1.0000 u 250.00 100.2
75-125 1272.4600 200.6100 1000.00 107.2
75-125 18.5000 2.0000 u 20.00 92.5
Magnesium
Manganese 75-125 537.5400 33.9700 500.00 100.7
Mercury 75-125 0.8660 0.2000 u 1.00 86.6
Nickel 75-125 495.9200 1.0000 u 500.00 99.2
Potassium
Selenium 75-125 12.0600 5.0000 u 10.00 120.6
Silver 75-125 53.0200 2.0000 u 50.00 106.0
M
p
p
p
p
p
p
NR
p
p
p
p
p
NR
p
CV
p
NR
p
p
. NR
75-125 51.4200 6.0000 u 50.00 102.8 p
Vanadium 75-125 504.7000 1.0000 u 500.00 100.9 p
75-125 508.4200 2.0000 u 500.00 101.7 p
NR
lmments:
' t
I
It
I FORM V (Part 1) -IN 000032 ILM04.0
I
U.S. EPA -CLP
5A I
It
EPA SAMPLE NO.
SPIKE SAMPLE RECOVERY
lf'ab Name: CHEMTECH CONSULTING
"r..ab Code: CHEM Case No.:
tatrix (soil/water):
% Solids for Sample:
SOIL
74.8
GROUP
25633
MDMP58S
Contract: 68-D5-0166
SAS No.: SDG No.: MDMP58
Level (low/med) : LOW
I Concentration Units (ug/L or mg/kg dry weight): MG/KG
Control " • Lirni-t Spiked Sample Sample Spike
Analyte %R -Result (SSR) C Result (SR) C Added (SA) %R Q
75-125 118.6497 1.2855 u 128.55 92.3
75-125 12.2583 1.9796 B 10.28 100.0
Barium 75-125 549.2004 69.3130 514.19 93.3
Beryllium 75-125 13.2841 0.6170 B 12.85 98.6
Cadmium 75-125 11.8881 0.2571 u 12.85 92.5
Calcium
romium 75-125 66.0839 16.0711 51.42 97.3
balt 75-125 127.9566 5.9466 B 128.55 94.9
75-125 71.7092 9.2452 64.27 97.2
56.2577 51.7585 5.14 87.5
Magnesium
Manganese 75-125 578.6508 460.0190 128.55 92.3
Mercury 75-125 0.7112 0.1337 u 0.67 106.1
Nickel 75-125 128.2960 6.7256 B 128.55 94.6
Potassium
Selenium 75-125 3.1880 1.2855 u 2.57 "124.0
.Silver 75-125 13.5181 0.5142 u 12.85 105.2
Sodium f halli"m 75-125 13.4513 1.5426 u 12.85 104.7
Vanadium 75-125 151.0721 24.0667 128.55 98.8
Zinc 75-125 169.7912 49.1670 128.55 93.8
Cyanide
Lmments:
! "t
I
'-I FORM V (Part 1) -IN 000032 ILM04.0
I
M
NR
p
p
p
p
p
NR
p
p
p
NR
p
NR
p
CV
p
NR
p
p
NR
p
p
p
NR
U.S. EPA -CLP
6
DUPLICATES
EPA SAMPLE NO.
MDLL03D fab Name: CHEMTECH CONSULTING GROUP
Lab Code: CHEM Case No.: 25633
Contract: 68-D5-0166
SAS No.: SDG No.: MDMP99
tatrix (soil/water): SOIL Level (low/med): LOW
% Solids for Sample: 36.8 % Solids for Duplicate: 36.4
I Concentration Units (ug/L or mg/kg dry weight): MG/KG
I
I
I
I ,
I
I
I
I
I
I
It
I
I
Analyte
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Cyanide
Control
Limit -.
4.0
79.3
2.0
19.8
9.9
1983.5
15.9
1983.5
2.0
Sample ( s) C Duplicate (D)
-55461.6630 56064.1860
3.2133 B 2.6936
5.1214 3.6338
228.9987 230.6490
2.6103 2.6539
0.3967 u 0.3967
1698.4330 B 1731.7955
62.9324 64.2098
22.1914 22.3699
41.5424 41.7645
44397.5484 45213.6584
46.4773 47.7745
4977.7253 5042.8951
627.3802 637.6388
0.2717 u 0.2717
27.4199 27.9078
4203.7686 4229.8159
2.8205 2.5746
0.7934 u 0.7934
300.2301 B 298.8416
3.0308 B 3.4434
105.0222 106.6249
133.2037 136.3020
-
FORM VI -IN
C RPD,. • Q M
--- -1.1 p
B 17.6 p
B 34.0 p
0.7 p
1. 7 p
u p
B 1.9 p
2.0 p
0.8 p
0.5 p
1. 8 p
2.8 p
1. 3 p
1.6 p
u CV
1.8 p
0.6 p
9.1 p
u p
B 0.5 p
B 12.7 p
1.5 p
2.3 p
NR
---
ILM04.0
000037
U.S. EPA -CLP
6
DUPLICATES
EPA SAMPLE NO.
MDMK13D lab Name: CHEMTECH CONSULTING GROUP
Lab Code: CHEM Case No.: 25633
Contract: 68-D5-0166
SAS No.: SDG No. : MDMP98
11atrix (soil/water): WATER Level (low/med): LOW
% Solids for Sample: 0.0 % Solids for Duplicate: 0.0
I
I
I
I
I ,.
Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
I
Analyte
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Cyanide
Control
Limit -.
5000.0
Sample ( s) C Duplicate (D) C RPD,. • Q M
-----180.8400 B 164.3800 B 9.5 p
5.0000 u 5.0000 u p
7.0000 u 7.0000 u p
24.2600 B 24.4200 B 0.7 p
1.0000 u 1.0000 u p
1.0000 u 1.0000 u p
5981.2400 6053.1500 1.2 p
3.0400 B 3.1400 B 3.2 p
2.0000 u 2.0000 u p
2.4200 B 2.2200 B 8.6 p
1306.0000 1309.6200 0.3 p
2.0000 u 2.0000 u p
2408.7800 B 2418.7600 B 0.4 p
347.1800 349.8300 0.8 p
0.2000 u 0.2000 u CV
2.8600 B 2.6800 B 6.5 p
1437.8000 B 1428.4600 B 0.7 p
5.0000 u 5.0000 u p
2.0000 u 2.0000 u p
4503.7400 B 4535.7600 B 0.7 p
6.0000 u 6.0000 u p
1.0800 B 1.0000 u 200.0 p
5.9200 B 3.4500 B 52.7 p
NR
----
FORM VI -IN 000048 ILM04.0
I
It
U.S. EPA -CLP
6
DUPLICATES
EPA SAMPLE NO.
MDMP63D rab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
SAS No.: Lab Code: CHEM Case No.: 25633 SDG No. : MDMP63
Jatrix (soil/water) WATER Level (low/med): LOW
% Solids for Sample: 0.0 % Solids for Duplicate: O. O
I Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
g
D
I
m
I
I
I
It
I
I
Analyte
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Cyanide
Control
Limit -.
100.0
15.0
Sample ( s) C Duplicate (D) C RPD,. .Q M -----55.5900 B 55.6000 B 0.0 p
5.0000 u 5.0000 u p
7.0000 u 7.0000 u p
29.7200 B 29.8100 B 0.3 p
1.0000 u 1.0000 u p
1.0000 u 1.0000 u p
4869.8400 B 4902.6000 B 0.7 p
1.0000 u 1.0000 u p
2.0000 u 2.0000 u p
1.0000 u 1.0000 u p
200.6100 193.1600 3.8 p
2.0000 u 2.0000 u p
2343.4400 B 2355.2400 B 0.5 p
33.9700 34.0200 0.1 p
0.2000 u 0.2000 u CV
1.0000 u 1.0000 u p
1036.1100 B 1035.3800 B 0.1 p
5.0000 u 5.0000 u p
2.0000 u 2.0000 u p
2542.3000 B 2543". 0400 B 0.0 p
6.0000 u 6.0000 u p
1.0000 u 1.0000 u p
2.0000 u 2.0000 u p
NR
--- -
FORM VI -IN 000033 ILM04.0
I
It
U.S. EPA -CLP
6
DUPLICATES
EPA SAMPLE NO.
MDMP58D ltab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
~ab Code: CHEM Case No.: 25633
tatrix (soil/water):
% Solids for Sample:
SOIL
74.8
SAS No.: SDG No.: MDMP58
Level (low/med): LOW
% Solids for Duplicate: 74.3
I Concentration Units (ug/L or mg/kg dry weight): MG/KG
I
D
I
I
I
I
I
I
It
I
I
Analyte
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Cyanide
Control
Limit -.
51.4
6.4
1285.5
1285.5
12.9
Sample (S) C Duplicate (D) C RPD,. • Q M
-----7042.2151 7083.9212 0.6 p
1. 2 855 u 1. 2855 u p
1.9796 B 1.7997 u 200.0 p
69.3130 69.6447 0.5 p
0.6170 B 0.6222 B 0.8 p
0.2571 u 0.2571 u p
455.6304 B 460.4741 B 1.1 p
16.0711 16.2845 1.3 p
5.9466 B 5.9466 B 0.0 p
9.2452 9.3609 1.2 p
12506.7462 12570.7014 0.5 p
51.7585 52.0953 0.6 p
1983.4430 1994.0971 0.5 p
460.0190 463.4461 0.7 p
0.1337 u 0.1337 u CV
6.7256 B 6.8285 B 1.5 p
2037.7160 2045.4391 0.4 p
1.2855 u 1.2855 u p
0.5142 u 0.5708 B 200.0 p
106.6382 B 106.2526 B 0.4 p
1.5426 u 1.5426 u p
24.0667 24.1901 0.5 p
49.1670 49.4472 0.6 p
NR
----
FORM VI -IN 000033 ILM04.0
U.S. EPA -CLP
7
LABORATORY CONTROL SAMPLE --·-
Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166 Jab Code: CHEM Case No.: 25633 SAS No.: SDG No. : MDMP9 9
Solid LCS Source: EPA-LV
lqueous LCS Source:
Analyce
Arsenic
Barium
Beryllium
Cadmium
gnesium
anganese
Mercury
Nickel
Potassium
'
Selenium
Silver
Sodium
I
I
I
hallium
inc
yanide
It
I
I
Aqueous (ug/L)
True Found ~R
Solid (mg/kg)
True Found C Limits
308.7 282.1 193.1 ,.:12,A . 2 91.4
213.3 203.6 129.4 -297_2 95.5
930.4 869.2 613.4 1247.2 93.4
5.3 5.0 B 2.5 8.1 94.3
18.8 16.5 15.3 22.2 87.8
41.6 34.8 32.1 51.1 83.7
184154.0 185245.2 142933.0 225376.0 100.6
96.5 84.2 77.8 115.2 87.3
140.3 117.7 115.4 165.6 83.9
6680.2 5978.1 5727.3 7633.1 89.5
21012.1 19982.1 16831.3 25193.0 95.1
224.1 175.l 167.6 280.5 78.1
' 113189. 0 99871.7 97493.0 128886.0 88.2
201.2 175.2 167.9 234.4 87.1
12.3 12.3 7.8 16.9 100.0
56.8 46.6 43.5 70.1 82.0
102.4 82.5 B 0.0 379.3 80.6
37.0 34.8 17.6 56.4 94.1
20.9 19.8 13.2 28.5 94.7
92.8 160.1 B 0.0 277. 4 172.5
38.1 33.9 24.6 51.6 89.0
65.8 55.8 53.0 78.6 84.8
174.9 140.0 127.7 222.1 80.0
FORM VII -IN ILM04.0
000038
U.S. EPA -CLP
7
LABORATORY CONTROL SAMPLE
Name: CHEMTECH CONSULTING GROUP Contract: lab Code: CHEM
llirolid LCS Source:
Case No.: 25633 SAS No.:
(queous LCS Source: EPA-LV
Analyte
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
d
nesium
otassium
Selenium
I
I
I
ilver
It
I
I
Aqueous (ug/L) Solid
True Found %R True Found
978.0 1060.32 108.4
4&5·. 0 557.90 115.0
SQ. 9 55.06 108.2
1004.5 1028.11 102.4
238.0 265.72 111.6
304.8 330.20 108.3
25355.5 26844.78 105.9
235.5 254.58 108.1
260.0 285.43 109.8
248.5 249.08 100.2
992.5 1126.62 113.5
2518.4 2745.73 109.0
12294.0 13479.52 109.6
245.5 261.96 106.7
248.5 259.01 104.2
24801.5 24312.66 98.0
50.7 56.96 112.3
295.0 312.97 106.1
24393.0 26640.14 109.2
49.4 57.58 116.6
246.0 266.33 108.3
1506.0 1698.34 112.8
FORM VII -IN
-. -
68-DS-0166
SDG No. : MDMP98
(mg/kg)
C Limits %R
,. •
000049
ILM04.0
I
-
U.S. EPA -CLP
7
LABORATORY CONTROL SAMPLE
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
lab Code: CHEM Case No.: 25633
liolid LCS Source:
'queous LCS Source: EPA-LV
Aqueous (ug/L)
Analyte
Barium
Beryllium
Cadmium
Calcium
nesium
otassium
Selenium
I
I
I
ilver
True
978.0
415-S-.0
50.9
1004.5
238.0
304.8
25355.5
235.5
260.0
248.5
992.5
2518.4
12294.0
245.5
248.5
24801.5
50.7
295.0
24393.D
49. 4
246.0
1506.0
Found %R
1053.36 107.7
557.38 114.9
55.52 109.1
1023.80 101.9
263.96 110.9
327.78 107.5
26647.40 105.1
253.48 107.6
283.67 109.1
247.90 99.8
1122.94 113.1
2736.26 108.7
13401. 68 109.0
260.80 106.2
257.20 103.5
24285.46 97.9
55.18 108.8
311.75 105.7
26464.92 108.5
57.44 116.3
265.08 107.8
1687.44 112.0
True
SAS No.:
Solid
Found
'-I FORM VII -IN
I
SDG No. : MDMP63
(mg/kg)
C Limits %R
" .-
()QGQ.34 ILM04.0
I '
U.S. EPA -CLP
7
LABORATORY CONTROL SAMPLE
Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166 I Lab Code : CHEM Case No.: 25633
Solid LCS Source: EPA-LV
.Aqueous LCS Source:
SAS No.: SDG No.: MDMP58
1,---------,-------.-------~
Aqueous (ug/L) Solid (mg/kg) Analyte I Aluminum
Antimony
I Arsenic
Barium
Beryllium
I Cadmium
Calcium
Chromium
Cobalt
gnesium
anganese
Mercury
Nickel
Potassium
Selenium
Silver
I
I
It
I
I
True Found iR True Found
308.7 321.3
213.3 205.1
930.4 929.1
5.3 5.7
18.8 17.7
41. 6 38.l
184154.0 170858.6
96.5 91.2
140.3 128.5
6680.2 6096.2
21012.1 21255.2
224.l 195.6
113189.0 102344.5
201.2 187.6
12.3 12.2
56.8 51. l
102.4 101.0
37.0 38.8
20.9 21.0
92.8 197.2
38.l 33.3
65.8 59.5
l 74. 9 158.2
FORM VII -IN
C Limits %R
193.1 '14 2'"4 . 2 104.1
129.4 297.2 96.2
613.4 1247.2 99.9
B 2.5 8.1 107.5
15.3 22.2 94.1 32.1 51.l 91.6 142933.0 225376.0 92.8 77.8 115.2 94.5
115.4 165.6 91.6
5727.3 7633.l 91.3 16831.3 25193.0 101.2
167.6 280.5 87.3 97493.0 128886.0 90.4
167.9 234.4 93.2
7.8 16.9 99.2
43.5 70.1 90.0
B 0.0 379.3 98.6
17.6 56.4 104.9
13.2 28.5 100.5
B 0.0 277.4 212.5
24.6 51.6 87.4
53.0 78.6 90.4
127.7 222.l 90.5
OOOC34 ILM04.0
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I
I
I
I
I
MEMORANDUM
Date: 10/15/97
Subject: Results of VOLATILES ORGANIC Sample Analysis
I ,
97-0328 JOHNSON CONTROLS GLOBE
WINSTON-SALEM, NC
From: John Mcconney r\,l~
To: PAT DEROSA
Thru: QA Office
RECEIVED
OCT 16 1997
SUPERFUND SECTION
Attached are the results of analysis of samples collected as part of the subject project. If you have any I questions, please contact me .
• ATTACHMENT
0
D
It
I
I
I
It
I
I
I
I
I
I
I
I
I
I
I
I
It
I
ORGANIC DATA QUALIFIER REPORT
Case
Site
Number 25633 Project Number 97-0328 SAS Number
NC ID. Johnson Controls Globe, Winston-salem,
Affected Samples
Volatiles
12413,12414,
12446,12448,
12450,12452,
12469,12473
12442
Extractables
12413, 12414,
12453,12455,
12458,12463,
12465,12466
12419
12424
12428
12445
12450
12467
12468
12469
Compound or Fraction
toluene
trichloroethene
all compounds
J
J
J
4-chloro-3-methylphenol J
4-nitrophenol J
2,4-dinitrotoluene J
pyrene J
4-methylphenol J
fluoranthene J
pyrene J
chrysene J
benzo(b/K)fluoranthene J
phenanthrene J
carbazole J
benzo(a)anthracene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
benzo(g,h,i)perylene J
acenaphthene J
f luorene J
anthracene J
carbazole J
dibenzo{a,h)anthracene J
f luoranthene J
pyrene J
benzo(b/k)fluoranthene J
phenanthrene J
carbazole J
dibenzo(a,h)anthracene J
acenaphthene J
dibenzofuran J
fluorene J
anthracene J
f luoranthene J
pyrene J
chrysene J
Flag
Used Reason
< quantitation limit
< quantitation limit
exceeded holding times
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitat:.on limit
< quantitat1.on limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
I
It
I
I
I
I
I
I
I
I
I
I
I
I
It
I
I
Affected Samples
13655
Pesticides
N/A
ORGANIC DATA QUALIFIER REPORT
Case Number 25633
Compound or Fraction
fluoranthene
Flag
Used
J
pyrene J
di-n-octylphthalate J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
dibenz(a,h)anthracene J
benzo(g,h,i)perylene J
Reason
< quantitation limit
< quantitation limit
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
recovery
recovery
recovery
recovery
recovery
recovery
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12462 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC001 SL .
Media: SOIL
RESULTS UNITS
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
40U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11 U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11 U UG/KG
11 U UG/KG
11U UG/KG
11 U UG/KG
11 U UG/KG
11 %
Case Number: 25633
D Number: MP70
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE(TETRACHLOROETHYLENE) ·
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:15
Ending:
A-average value. NA-not analyzed. NAl-interierences. J-estimated value. N-presumptive evidence of presence of material.
K-actua. I vallJe is known to be less than value given. L-actual value is known to be greater than value giv~U-material was analyzed for but not detected. the number is the minimum qu;J/lnli limit.
R-qc indicates 1~:1,Aunusable. compound may or may not be present. resampling and reanalysis is sary for verification. ·
C-co-d by tll!Jrw-valu.,orte-chlor-onst-2.c.ents -•be ech-lord'IIII --all 1!!11 == liliiil
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12463 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC101 SL
Media: SOIL
RES UL TS UNITS
11U UG/KG
11 U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11 U UG/KG
11 U UG/KG
11 U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
12 %
Case Number: 25633
D Number: MP71
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-a~tual value is known to be greater than value giv~U-material was analyzed for but not detected. the number is the minimum qu;,,nti · limit.
R-qc indicates t~:~nusable. com~ound may or may not be presen_t. resampling ~nd reanalysis is sary for_ verification.
C-co-d by IIW'w-valufM'orte\ilichlorlllltonst-2.c.ents -•b ech-lord'lall --a!!!!!!I !11!1 ;m
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12463 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC101 SL
Media: SOIL
RES UL TS UNITS
6JN UG/KG
D Number: MP71
ANALYTE
DIMETHYL SULFIDE
Org Contractor: COMPU
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estirnated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value giv~-material was analyzed for but not detected. the number is the minimum qu;,,n · limit.
R-qc indicates tha;Aunusable. compound may or may not be present. resampling and reanalysis is sary for verification. ·
C-c-d by ll!!IJIII" wli!I' val-port"(l!l!!I chlo[t!!!!!!l°ons\'W 2."!lll'ents-tab tech'Iilll'lord----l!!!!!!!!I !!!!!!IS
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12464 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC003SL
Media: SOIL
RESULTS
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
25
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MP72
ANALYTE
CHLOROMETHANE
BROM OM ETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 18:30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number 1s the minimum q";/lanf n hm1t
R-qc indicates I~-unusable. compound may or may not be present. resampling and reanalysis i~~ary for verification.
C-c-d by •. w .. o valurWiiporteflii chlo.cons-2.c.uents-ta~ tech-lord-... --1111!1 l!!!!I
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12465 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC004SL
Media: SOIL
RESULTS
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
39
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MP73
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:45
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number 1s the minimum quant-l1m1t ~:i~a·~)~";~iiv~~ueJF~r0~=1°:·s%1~~H2rr~~~~ri:irfi~p~0r1rur~~=~;~-~c~1'ii:'Fr~~~.. ---. I!!!!! ,,., -= rm
VOLATILES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA
Sample 12466 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC00SSL
Media: SOIL
RESULTS UNITS
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11 %
D Number: MP7 4
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COM PU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:00
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value giv~U-material w. as analyzed for but not detected. the number is the minimum qu;,,nti · limit.
R-qc indicates t~~t.nusable. compound may or may not be present. resampling and reanalysis is sary for verification.
C-c-d by li!!!!!ll"·w\M' val-port"ll!!l!I chlo-ons-2 .• ents-tab 'tech.,lord-•-11111 -I!!!!! !!!!I
VOLATILES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA
Sample 12467 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC006SL
Media: SOIL
RESULTS
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
36
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MP75
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analYzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:00
Ending:
R-qc indicates t~:_t_anusable. compound may or may not be present. resampling and reanalysis is sary for verification.
K-actual value is known to be less than value given. L-actual value is known lo be greater than. value giv-U-material was analyzed for but not detected. the number 1s the mm1mum qu3ntl · limit
C-corfirmed by llial'whM valu-ortelliiichlor-onst-2.c.ents_.ab ech~lord'IIII -l!!!!I 11111!1 1!!11 liiiiil
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12468 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC007SL
Media: SOIL
RESULTS
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
20
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MP76
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-eslimated value. N-presumptive evidence of presence of material.
K-actual value is known to be tess than value given. L-actual value is known to be greater than value given. U-materiat was analyzed for but not detected. the number 1s the minimum qu:,,nt1 n J1m1t
R-qc indicates th~t unusable. co.mpound may or may not be present. resampling and reanalysis i~sary for verification.
C-confirmed by g .when no value is reporter: see chlordane const-i e 2.constituents or meta techJJ.iwlLci,lord~ l!l!!!I ----
11!!!!!!1 -,_ 11!!!!!!!1 -,.. ---........ --
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12469 FY 1997 Project: 97-0328
VOL.ATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC008SL
Media: SOIL
RES UL TS UNITS
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11 U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
2J UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
7 %
D Number: MP??
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
. ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1 ,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:35
Ending:
R-qc indicates t~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actuat value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number 1s the minimum qu;Jfn n limit.
C-confirmed by il!!!!P" .w. valu-ortelll!!i chlo-cons-2 .• ents-a techlii!lflord-1!!!!11 == liiiiiii ---
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12470 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC009SL
Media: SOIL
RES UL TS UNITS
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11 U UG/KG
9 %
Case Number: 25633
D Number: MP78
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John McConney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 21 :45
Ending:
R-qc indicates th a A unusable. compound may or may not be present. resampling and reanalysis i sary for verification. ·
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum qu;Jln · limit.
C-c-d by 11!1111' .w. valu!M'orte-chloltllfons-2.c.ents-ab tech,..,lordl!!!!!l!!l !!!!I 1:ii:11 liiiiiil iiiil --
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 13655 FY 1997 Project: 97-0328
VOL.ATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC010SL
Media: SOIL
RESULTS
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
21
UNITS
UGIKG
UGIKG
UGIKG
UGIKG
UG/KG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UG/KG
UG/KG
UGIKG
UGIKG
UG/KG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MP65
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1,1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. N_A-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT OEROSA
Project Leader: OEROSA
Beginning: 08113197 17:20
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum q;Jjant n limit
R-qc indicates t~-unusable. compound may or may not be present. resampling and reanalysis iAss_ary for verification.
C-c-d by tfllll// .when no valu-porte!Wi chlo-cons-2 .• entsMta~ tech-lordillilll!I l!!!!!!!I l!!!!!!!!I 1!!!!!!11 =:; --
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12455 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program·: NSF Case Number: 25633
Id/Station: JC011 SL MD Number: MP66 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SOIL
RESULTS UNITS
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
23 %
D Number: MP66
ANALYTE
CHLOROMETHANE
BROM OM ETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1;1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analYzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 16:25
Ending:
R-qc indicates !~~-unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~ive LI-material was analyzed for but not detected. the number 1s the mm1mum qu;J/lnt limit
C-c-d by ~-w-valu-orteilill chlo-cons-2 .• ents-tab tech'iall"lord-l!!!!!!!!I l!Zi:I =i:;; liiii --
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12456 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC012SL MD Number: MP67 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SOIL
RESULTS UNITS
14U UG/KG
14U UG/KG
14U UGIKG
14U UGIKG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UGIKG
14U UG/KG
14U UG/KG
14U UGIKG
14U UGIKG
14U UGIKG
14U UG/KG
14U UGIKG
14U UGIKG
14U UGIKG
14U UGIKG
14U UGIKG
14U UGIKG
14U UGIKG
14U UGIKG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
28 %
D Number: MP67
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08113197 17:56
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-act~al.value is known to be less than value given. L-actual value is known to be weater than valu~ ~~iv Li-material w~~ a~alyzed for but not detected. the number is the minimum q;;/lan · · n limit.
R-qc md1cates t~-unusable.· compound may or may not be present. resamplmg and reanalysis I ssary for veriflcatron.
C-c-dbyill"w/N'valwport-chlo-cons-2-ent .. ta tech.,lord--l!!!!!!!!l i!!!!!!1 == iiii -
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12444 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC013SL MD Number: MP54 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SOIL
RESULTS UNITS
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
21 %
D Number: MP54
ANALYTE
CHLOROMETHANE
BROM OM ETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETH.ENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :50
Ending:
R-qc indicates t~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value gliiv. U-material was analyzed for but not detected. the number 1s the minrmum q;Jlan n 11m1t
C-crfirmedbylil!!l',.w.oval-port'Mchl-con-s 2 .• uent-ta tech-hlora -I!!!!!! !!!! 1!11!!1 rm iliii
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12445 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC014SL
Media: SOIL
RESULTS
12U
12U
12U
12U
12U
12U
20U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
17
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
Case Number: 25633
MD Number: MP55
D Number: MP55
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NA1-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 15:45
Ending:
R-qc indicates th. unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv LI-material was analyzed for but not detected. the number is the minimum q;;,,an · · n limit.
C-c-d by~ .w. val'll!!!i!lport'!iM chl'\1111constlllf' 2 . .,ent,..ta tech-hlord---. l!!!!!!!!!I l!!!!!!I ;;;;; iiii
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12442 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC001 SW MD Number: MP52 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA D Number: MP52
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UG/L
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
9J UGIL
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UGIL
10U UGIL
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13197 11 :00
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presurnptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g-ive Li-material was analyzed for but not detected. the number 1s the minimum q;J/lant n hmat
R-qc indicates 1~:aunusable. compound may or may not be present. resampling and reanalysis i -sary for verification.
C-c-d by tl!!lll'_w_ val-portiilll chlo-consw 2 .• ent,.ta tech-hlord------
VOLATILES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA
Sample 12443 FY 1997 Project: 97 -0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC001 SD
Media: SEDIM
RESULTS
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
41
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
Case Number: 25633
MD Number: MP53
D Number: MP53
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presurnptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-materiat was analyzed for but not detected. the number 1s the minimum q;;J/lan n limit
R-qc indicates~~-unusable. compound may or may not be present. resampling and reanalysis i-s~ary for verification.
C-caed byrf///!IIT .when no val .. porty, chi-con-s 2 .• uent,.ta~ tec-hlor. ------
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12447 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC002SW MD Number: MP57 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: MP57
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Lea.der: DEROSA
Beginning: 08/13/97 19:45
Ending:
R-qc indicates th-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number 1s the minimum qu~n n limit
C-c-d by~, wll!I' val1ilport,W chlol!!!!!l°ons!M 2 .• ent"Mta techlillllltlord-------
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12446 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC002SD MD Number: MP56 lnorg .Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS UNITS
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
2J UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
35 %
D Number: MP56
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,<1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1 ,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 12:30
Ending:
A-average value. NA-not analyzed. NAl-interierences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value ls known to be greater than value g~iv. U-material was analyzed for but not detected. the number 1s the minimum q~a n J1m1t
R-qc indicates t~--unusable. compound may or may not be present. resampling and reanalysis · ssary for verification.
C-c-ed byll!!!!!ll''-w-vailiifport'llliil chic-con'Ms 2 .• ent'Mta tech-hlord------
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12448 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC003SD MD Number: MP58 lnorg Contractor: CHEM
Org Contractor: COM PU Media: SEDIM
RESULTS
14U
14U
14U
14U
14U
14U
30U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
2J
14U
14U
14U
14U
31
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MP58
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROM OF ORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :15
Ending:
R-qc indicates !~~-unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-actual value is known to be less than value given. L-actuar value is known to be greater than value g-ive LI-material was analyzed for but not detected. the number 1s the minimum qu;,,nt n hm1t
C-co-d by_ ii!!!!!ll'.w'/M valuliii!!i'orte1-chlo-ons\M 2 °tii!renls -• tech'lllll'lord------
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12449 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC004SW MD Number: MP59 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA D Number: MP59
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
CHLO ROM ETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 10:05
Ending:
A-average value. NA-not analyzed. NAl-interterences. J-estimated value. N-presumptive evidence of presence of material.
K-ac. tua! value is known lo be less than value given. L-actual value is known to be great~r than value g~·v U-material was analyzed for but not detected. the number is the minimum q";Jlan · · n limit.
R-qc indicates t~a_A unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-c-d bylia'.wM val-port1'1 chl°JMconsM 2 . .,ents-ta tech,..,lord-------
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12450 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC004SD
Media: SEDIM
RESULTS
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
2J
17U
17U
17U
17U
41
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
Case Number: 25633
MD Number: MP60
D Number: MP60
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Projecl Leader: DEROSA
Beginning: 08/13/97 10:30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g-iv LI-material was analyzed for but not detected. the number is the minimum q;llan · limit.
R-qc indicates thaA unusable. compound may or may not be present. resampfing and reanalysis i ssary for verification.
C-c-dbyiii91"·11ifval'llifportlillfchl'11111con-s 2 .• uent,_ta teci-..hlor'911 ------
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12451 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC005SW MD Number: MP61 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA
RES UL TS UNITS
10U UGIL
10U UGIL
10U UGIL
10U UGIL
10U UGIL
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UGIL
10U UG/L
D Number: MP61
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08113197 12:05
Ending:
R-qc indicates t~-unusable. compound may or may not be present. resampling and reanalysis i ~sary for verification. .
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum qu;,,n · · n limit.
C-co-dby~.w-valu-orte-chlo-ons-2.caenls-a tech'llllflord-------
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12452 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC005SD MD Number: MP62 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
2J
15U
15U
15U
35
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MP62
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1,1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 12:35
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv LI-material was analyzed for but not detected. the number is the minimum q;//Jan · · n limit.
R-qc indicates t~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-c-dbyllll".w-val-port-chl-cons-2 .• ent .. ta tech-hlord-------
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12422 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC006SW MD Number: MH94 I norg Contractor: CH EM
Org Contractor: COMPU Media: SURFACEWA D Number: MH94
RESULTS-UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U . UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 12:25
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g-ive U-material was analyzed for but not detected. the number is the minimum q:,,ant" · n limit.
R-qc indicates t~:-unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-c-dby~.w-valwport'aiichl-con-s 2 .• ent'Mta tech-hlord-------
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12423 FY 1997 Project: 97 -0328
VOLATILES SCAN
Facility: JOHNSON.CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC106SW MD Number: MH95 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
D Number: MH95
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 12:30
Ending:
R-qc indicates tha-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum qu;;J/ln · · n limit._
C-c-d bytaJ.w-val-port-chl'1illconsW 2.,ents-ta techlilW'lord-------
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12424 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC006SD MD Number: MH96 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS
42U
42U
42U
42U
42U
42U
270U
42U
42U
89
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
76
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MH96
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08112197 13:00
Ending:
A-average value. NA-not analyzed. NAl-interfei-ences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g-ive U-material was analyzed for but not detected. the number is the minimum q;,,anr · limit.
R-qc indicates t~~-unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-c-dby~.w-val'ililiportwchlo-cons-2 .• ent .. ta tech.,lord------
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12434 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC007SW MD Number: MK09 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA D Number: MK09
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENE$
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:26
Ending:
R-qc indicates thaA, unusable. compound may or may not be present. resampting and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum q;fjan.· · n limit.
C-c-d by,ai,i.ww val-port-chl-con'illlllls 2 . ..,ent'fMta tech-hlord--II!!!! --1!!!!!!!1 I!!!!!
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12436 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC107SW
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
40U
10U
10U
10U
10U
·10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
Case Number: 25633
MD Number: MK11
D Number: MK11
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:26
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number ts the minimum qu>nt n 1Jm1t
R-qc indicates t~~ unusable. compound may or may not be present. resampling and reanalysis i:Ass_ary for verification.
C-co.d by iil!l'.w-valu-orteWiichlor-ons-2.c.enls·•~lech-lord------
' -
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12435 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC007SD MD Number: MK10 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS
30U
30U
30U
30U
30U
30U
100U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
67
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MK10
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:55
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number 1s the minimum q";ljant n llm1t
R-qc indicates t~-unusable. compound may or may not be present. resampling and reanalysis i·s~ary for verification.
C-c~d by r!i!!/f!!l1 .w. valu-porteii!li ch lo-cons-2 .• ents-ta~ tech-lordiilll -----~
I
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12438 FY 1997 Project: 97-0328
VOLATILES SCAN ·
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC008SW
Media: SURFACEWA
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
Case Number: 25633
MD Number: MK13
D Number: MK13
ANALYTE
CHLOROMETHANE
BROM OM ETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 19:25
Ending:
R-qc indicates th,a. unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~·v LI-material was analyzed for but not detected. the number is the minimum q;flan · n limit.
C-c-d bl\i!!!!!!IIJ" ·,W, valll!i!fportM' chl'M con'!llllls 2 .• uent,..,ta tec~hlorcmi. -----. ' .
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12437 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC008SD MD Number: MK12 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS
15U
15U
15U
15U
15U
15U
30U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
34
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MK12
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
· Ending:
R-qc indicates ~~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum q;,,an · · n limit.
C-c-d byd!i!!!!!!II', ·'1i!!!!!f val•.,port'M' chi-con'Ms 2 liliuent'ialfta tec111111hlor'111111 ------
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12439 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC108SD MD Number: MK14 lnorg Contractor: CHEM
Org Contractor: COM PU Media: SEDIM
RESULTS
15U
15U
15U
15U
15U
15U
40U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
33
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MK14
ANALYTE
CHLO ROM ETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAJ-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
K-actual value is known to be less.than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number 1s the minimum qu;,,n n l1m1t
R-qc indicates t~-unusable. com~ound may or may not be presen_t. resampling ~nd reanalysis i-s~ary for_ verification.
C-col!l!lt by ~ •. wti!li valu-porteii!iii chlo-cons-2.c.entsiiita~techwlord'IMII ------
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12441 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC009SW MD Number: MP51 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA D Number: MP51
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
R~questor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:45
Ending:
R-qc indicates t~--unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv. U-material was analyzed for but not detected. the number 1s the m1mmum qu;/ln n limit
C-c°Cfirmedbyl!!l",.w.valu-,ortelliichlo-ons-2.c.ents-a tech'llillilord------
' --
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12440 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program' NSF Case Number: 25633
Id/Station: JC009SD MD Number: MP50 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS
20U
20U
20U
20U
20U
20U
60U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
51
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MP50
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actuaf value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum qu;J#nt' limit.
R-qc indicates thaA unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-c-d by !11111' ·w'M valu-ortell!!!!M chlo,.,ons'n!!Mf 2 cll!!!!!lents 11!!!!11• tech'lll!lflord-------
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12453 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC010SW MD Number: MP63 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: MP63
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 09:40
Ending:
R-qc indicates t~a-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actua. I value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum qu;,,nr · n limit.
C-c-d by ti!!!!!!!!'° .w\'M valu-orteliJIMI chloM"ons-2 . .,ents-ta tech'lilif lord-------
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12454 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC01 0SD MD Number: MP64 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
24
UNITS
UG/KG
UG/KG
UG/KG
UG/KG.
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MP64
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John McConney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 09:25
Ending:
R-qc indicates thaA unusable.· compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual.value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number 1s the m1n1mum qu;,,nt 11m1t
C-c-·d by 11!!!!111" w'!M valu!M'ortell!!!!I chloli!l!lfons'JM 2.'lllllrents-a tech~lord------I!!!!!!!!
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12429 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC011 SW
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
Case Number: 25633
MD Number: MJ01
D Number: MJ01
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:25
Ending:
K-actual value is-n wn to be less than value given. L-actual value is known to be greater than value g~i U-material was analyzed for but not detected. the number is the minimum qu";Jln · · n limit.
R-qc indicates th unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-c.,d by ,w\'M valu~orte-chlo(M'ons-2 ~•nts-a tech'Jlll'lord-------
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12430 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC011 SD
Media: SEDIM
RESULTS UNITS
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
40U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
34 %
Case Number: 25633
MD Number: MJ02
D Number: MJ02
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interterences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
R-qc indicates t~a-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum qu~n · · n limit.
C-co-dby~.w-valu'fM'orte\llllchlor-onst-2.c.ents-a ech,_lord,.. -----
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12420 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC012SW MD Number: MH92 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: MH92
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08112/97 11 :12
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value gflll;iv U-rnaterial was analyzed for but not detected. the number is the minimum qu;/ln · limit.
R-qc indicates Iha-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-c-dbylJIIIP.w-valu_,orte-chlo.,ons ... 2."IIIIIM'ents-ta tech,..,lord-------
VOLATILES SAMPLE ANft,L YSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12421 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC012SD MD Number: MH93 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM D Number: MH93
RES UL TS UNITS
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U . UG/KG
SOU UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
33 %
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptlve evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 11 :30
Ending:
R-qc indicates Iha-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum qu;J/ln · · limit.
C-c-dbyllllll'w-valwport-chlo-cons-2.~ents-ta tech..,,lord-------
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12431 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC013SW MD Number: MK06 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA D Number: MK06
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:35
Ending:
R-qc indicates t~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~ive. LI-material was analyzed for but not detected. the number 1s the mrnimum qu";J/lnt n hm1t
C-c-d by r1flll' .w. vall-port"Iilii chlo-cons-2 .• ents-ta techiiillr'lordt!!!!l!!!I !!!!!I l!!!I!! 1!!!!11 ISllm _ liiiil iiiil
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12432 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC013SD
Media: SEDIM
RESULTS UNITS
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
27 %
Case Number: 25633
MD Number: MK07
D Number: MK07
ANALYTE
CHLOROMETHANE
BROM OM ETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENE$
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estlmated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:50
Ending:
R-qc indicates t~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv .. U-materiaf was analyzed for but not detected. the number is the minimum qu";J/ln · · n limit.
C-cotii!ir by 111111' .w. val-port-chlo-cons-2 .• ents-ta tech.,lordill!!I l!!!!!!!I 11!!!!1 ml!!! 1:1 -liiii -
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12419 FY 1997 Project: 97 -0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC0 14SW
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
. UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
Case Number: 25633
MD Number: MH91
D Number: MH91
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:45
Ending:
K-actual value is known to be less than value given. L-actua1 value is known to be greater than value g~i U-material was analyzed for but not detected. the number is the minimum qu";//jn · · n limit.
R-qc indicates Iha-unusable. compound may or may not be present resampling and reanalys.is i ssary for verification.
C-c-d by 19' w-valuflilf'orte-chlo-ons-2c-entsdl!!Wa tech'!!!l!i!i1lord'!!II i=:I liliiil liiiil ---
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12418 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC014SD MD Number: MH90 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS
23U
23U
23U
23U
23U
23U
30U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U 23U.
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
56
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG ·
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MH90
ANALYTE
CHLOROMETHANE
BROM OM ETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Production Date: 10/15/97 08:25
Produced by' John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:33
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv LI-material was analyzed for but not detected. the number is the minimum qu;Jln · limit.
R-qc indicates Iha.unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-c-d by ~.w. valu-orteM chloll!lfons'IM 2 .• ents-ta tech'i!!!!!!!!i11ord'l!!!!!!!!!I 11!!!!!!1 1111!1 ---
------------. _--. . . . . -. . . . . . . . .
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12427 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC015SW MD Number: MH99 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
D Number: MH99
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 11 :47
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum qu;Jint n 11m1t
R-qc indicates !~~-unusable. compound may or may not be present. resampling and reanalysis i~s_ary for verification.
C-confirm~d by ... w. valu-porte/W chlo-cons-2 .• ents-ta~techwlord---11!!!!!!1 !!!!Ill ~
' '. I: • -, .
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12428 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC015SD MD Number: MJ00 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS UNITS
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
40U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
45 %
D Number: MJ00
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1,1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 12:15
Ending:
R-qc indicates tha\Aunusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv Li-material was analyzed for but not detected. the number is the minimum qu;,,nr · limit.
C-co-d by iia'·wll!l!!!i valu-orteilllchlo.,onsiia 2.c.ents-a tech"ll!!!!li11ord'ma i= liiiiiiii iiiiil ---
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12433 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC016SD MD Number: MK08 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
32U
69
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MK08
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROM OF ORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 15:35
Ending:
R-qc indicates Iha-unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum qu~n · · n limit.
C-co-d by ii11'·w7M valuiiliil'ortelllilichlo'!Mtonstllr 2 . .,.ents .l!!!!!!i• ech1!!!!!!!1lord~ i:= lilail liliiiil liiii --
VOLATILES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA
Sample 12425 FY 1997 Project: 97 -0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC017SW MD Number: MH97 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
D Number: MH97
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (fRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (fETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estlmated value. N-presumptive evidence of presence of material.
K-a'ctual_value is known to be less than value given. L-actual value is known to be weater than valu~ ~iven. LI-material w~s a~alyzed.for but not detected. the number ts the minimum quu:,,n n llmit.
R-qc indicates t~~ unusable. compound may or may not be present. resamp!mg and reanalysis 1-s~ary for venficat1on. C-cooliit by 11111".w. valu-ortetlli!i chlofMl°ons-2.c.ents_a,....tech-lord--l!l!!!!!!I l!!l!!!I ll!l!i!! ==
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12426 . FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC017SD MD Number: MH98 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS UNITS
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
20 %
D Number: MH98
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:40
Ending:
R-qc indicates Iha.unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv LI-material was analyzed for but not detected. the number is the minimum q;,,an · · n limit.
C-c-d bylll!!!lll'.w!M' val-port-chl"lilllcons .. 2 . ..,ent'illltab techi!!!!!!hlordl!!!!!!!I 1!!!!11 i=;;a liiiiil ---
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12412 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC018SW MD Number: LL02 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA D Number: LL02
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 16:32
Ending:
R-qc indicates Iha.unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum qu";/ln · · n limit.
C-c-d by~ w\M val"Mi!ll'orte-chlo.,ons-2.'Jla'entsll!!!!!lta tech1!!!!!51lordt=II liili -----
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12413 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case.Number: 25633
Id/Station: JC018SD MD Number: LL03 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
28U
4J
28U
28U
28U
28U
64
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: LL03
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLO RO ETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 17:35
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g-ive. U-material was analyzed for but not detected. the number 1s the minimum q";Jjan n limit
R-qc indicates t~:-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-c-d by ~.w. valu-portetiliii chlo[ijjifons-2 .• ents11191a tech.,lord==a liiilil -----
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12414 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC019SD MD Number: LL04 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U .
24U
4J
24U
24U
24U
24U
58
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: LL04
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/9717:50
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv LI-material was analyzed for but not detected. the number is the minimum q;/lan · · n limit.
R-qc indicates t~a--unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-c-d byia," ·iiif val-port-chi-con-s 2 ilt'ent'iill!!fta tech!!!!llhlor~ a;a iiii ----
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12415 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC020SW MD Number: LL05 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UG/L
UG/L
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UG/L
UG/L
D Number: LL05
ANALYTE
CHLOROMETHANE
BROM OM ETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON.DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08111197 15:00
Ending:
R-qc indicates thaA. unusable. compound may or may not be present. resampling and reana_lysis i ssary for verification. _
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~i LI-material was analyzed for but not detected. the number is the minimum qu~· n limit. C-co-by 1:9'·w-valu-orte-chlor-onst-2.c.entsl!!l!!!!lia ech._lordiiii&I ------
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12416 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC021SW MD Number: LL06 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA D Number: LL06
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS.
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
CHLO ROM ETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NA1-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 17:00
Ending:
R-qc indicates tha-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv. U-materiaf was analyzed for but not detected. the number is the minimum q;;JJJan · · n limit.
C-c-d byll9' w-val-port-chi-cons-2 . ..,ent'il!!lfta techl!!!!!!lf11ord=a lililil iiiil ----
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12417 FY 1997 Project: 97 -0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC021 SD MD Number: MH89 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS
24U
24U
24U
24U
30U
24U
140U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
59
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MH89
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 18:40
Ending:
R-qc indicates 1~:1-unusable. compound may or may not be present. resampling and reanalysis is sary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value giv •. U-material was analyzed for but not detected. the number 1s the m1n1mum qu;,,nt n hmit
C-co.d by rw-w• valu-orte-chlor-onst-2.c.ents -ab echrmlord'= =a iili ----
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12457 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC001 PW MD Number: MP68 lnorg Contractor: CHEM
Org Contractor: COMPU Media: GROUNDWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: MP68
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:15
Ending:
R-qc indicates th a A unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv LI-material was analyzed for but not detected. the number is the minimum q;flan · · n limit.
C-c-d byflllll' .w. val-port-chl'1111cons .. 2 . ..,ent'tll!Jta tech19!!hlordll!II i=! ;;;a iiiiil ---
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12458 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC002PW MD Number: MP69 lnorg Contractor: CHEM
Org Contractor: COMPU Media: GROUNDWA
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
D Number: MP69
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John McConney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 21 :00
Ending:
R-qc indicates Iha-unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-a.ctual value is known to be less than value given. L-actual value is known to be greater than value g~iv Li-material was analyzed for but not detected. the number is the minimum q";J/lan · · n limit.
C-c-d by f!IIII' .w_ val-port-chlo-consw 2 . .,enls-ta tech'll!!!i'lordm== =-1iiii iiil ---
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12471 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC001TB
Media: WATER
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
D Number: MP79
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10115197 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 13:45
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number 1s the minimum q3'an on hm1t
R-qc indicates I-unusable. compound may or may not be present. resampling and reanalysis i-s~ary for verification.
C-confirmedby .whennovalu.port~chlo-cons-s 2 .• uents-ta~techliitlordllll -----
-11!!!1 . -
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12472 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC002TB
Media: WATER
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
Case Number: 25633
D Number: MP80
ANALYTE
CHLOROMETHANE
BROM OM ETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 13:45
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-eslimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value. g~iv U-material was analyzed for but not detected. the number is the minimum qu;Jin · · n limit.
R-qc indicates !~a-unusable. compound may or may not be present. resampling and reanalysis i _sary for verification. _
C-co-by 1111' w-valu-orte-chlor-onstM 2.c.ents !!If• ech'lll:i'lord'\=i lliiiia iiiiiii liiil ---
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12473 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC003TB
Media: SOIIL
RES UL TS UNITS
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
40U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
2J UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
4 %
D Number: MP81
ANALYTE
CHLOROMETHANE
BROM OM ETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 07:30
Ending:
A-average value. NA-not analyzed. NAl-interierences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known lo be greater than value g~iv LI-material was analyzed for but not detected. the number is the minimum qu;J/in · · n limit.
R-qc indicates Iha-unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-c-d by i.-, w-val-porte-chlo.,ons-2.reents-a techi;;i;f11ord'liliii iiii -----
I
It
I
I
I
I
I
I
1?a;/-·!,Jlj;,~) 4----
1 ' -
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
MEMORANDUM
Date: 1 0/15/97
Subject: Results of EXTRACTABLES ORGANIC Sample Analysis
97-0328 JOHNSON CONTROLS GLOBE
WINSTON-SALEM, NC
From: John Mcconney
To: PAT DEROSA
Thru: QA Office
RECEIVED
OCT 16 1997
SUPERFUND SECTION
Attached are the results of analysis of samples collected as part of the subject project If you have any
lquestions, please contact me.
I
I
.TTACHMENT
I
D
'-I
[1
I
I
I
I
I
I
B
I ,
I
I
I
I
'9
I
I
ORGANIC DATA QUALIFIER REPORT
Case Number 25633 Project Number 97-0328 SAS Number
NC Site ID. Johnson Controls Globe, Winston-salem,
Affected Samples
Volatiles
12413, 12414,
12446,12448,
12450,12452,
12469,12473
12442
Extractables
12413, 12414,
12453,12455,
12458,12463,
12465,12466
12419
12424
12428
12445
12450
12467
12468
12469
Compound or Fraction
toluene
trichloroethene
all compounds
J
J
J
4-chloro-3-methylphenol J
4-nitrophenol J
2,4-dinitrotoluene J
pyrene J
4-methylphenol J
fluoranthene J
pyrene J
chrysene J
benzo(b/K)fluoranthene J
phenanthrene J
carbazole J
benzo{a)anthracene J
benzo(b/k)fluoranthene J
benzo (a) pyrene J
indeno(l,2,3-cd)pyrene J
benzo(g,h,i)perylene J
acenaphthene J
f luorene J
anthracene J
carbazole J
dibenzo(a,h)anthracene J
fluoranthene J
pyrene J
benzo(b/k)fluoranthene J
phenanthrene J
carbazole J
dibenzo(a,h)anthracene J
acenaphthene J
dibenzofuran J
fluorene J
anthracene J
fluoranthene J
pyrene J
chrysene J
Flag
Used Reason
< quantitation limit
< quantitation limit
exceeded holding times
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< guantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< guantitation limit
< quantitatlon limit
< quantitation limit
< guantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
0
Affected samples
13655
D
D
I Pesticides
N/A
I
I
I
I
I
I
I
I
ORGANIC DATA QUALIFIER REPORT
case Number 25633
Compound or Fraction
Flag
Used
fluoranthene J
pyrene J
di-n-octylphthalate J
benzo(b/k)fluoranthene J
benzo{a)pyrene J
indeno(l,2,3-cd)pyrene J
dibenz(a,h)anthracene J
benzo{g,h,i)perylene J
Reason
< quantitation limit
< quantitation limit
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
recovery
recovery
recovery
recovery
recovery
recovery
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12462 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC001 SL
Media: SOIL
RESULTS
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
930U
370U
370U
370U
370U
370U
370U
930U
370U
930U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG ·
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MP70
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2.4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
Org Contractor: COMPU
RESULTS
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
930U
370U
930U
930U
930U
930U
370U
11
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:15
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-est[mated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv Li-material was analyzed for but not detected. the number is the minimum q;,,an · · n limit.
R-qc indicates thaA unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-c-d byi!!!J!!J" .w. val-port-chl"f!!!!!lcon5ms 2.,.,ent'Gfta tech-hlordi;;;; liiliiil liiliiil CIiia la lii&I liiiil
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12462 FY 1997 Project: 97 -0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC001 SL
Media: SOIL D Number: MP70 Org Contractor: COMPU
RESULTS UNITS ANALYTE
400J UG/KG 1 UNIDENTIFIED COMPOUND
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimaled value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than v. alue giv~-material wa.s analyzed for but not detected. the number is the minimum qu;,,nt: limit.
R-qc indicates !ha-unusable. compound may or may not be present. resampling and reanalysis is sary for verification.
C-co9d by ii!II' w'i!!!!5 vali'@!!l'orte-chlo'll!!!!fons~ 2 '1l!!lll'entsllll!!ab tech'l!!!!!!!!'lord'\!!!!!!I 11!!!!1 1!!!9 11!!!!!!1 la 111!!1 11!!!!!!!!1
EXTRACT ABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12463 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC101 SL
Media: SOIL
RESULTS
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
940UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
940UJ
370UJ
940UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MP71
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
EXCESSIVE HOLDING TIME
Org Contractor: COMPU
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:15
Ending:
RESULTS UNITS ANALYTE
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
940UJ
370UJ
940UJ
940UJ
940UJ
940UJ
370UJ
12
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual_value is known to be less than value given. L-actual value is known to be weater than valu~ ~~iv Li-material w~s a~alyzed for but not ~elected. the number is the minimum qu;/ln · limit.
R-qc indicates thaAunusable. compound may or may not be present. resamplmg and reanalys1s I sary for verification.
C-co-d by iliiiiiir.w-valiaiiiir'orteliiii chlo.=,:ons-2.'lillla'ents~ab tech_,lord,lii:m l==i 1111111 l!!!!!I 11111 l'll!!!ll l!!l!!!I
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12463 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC101 SL
Media: SOIL
RES UL TS UNITS
1 0000J UG/KG
S000J UG/KG
D Number: MP71
ANALYTE
7 UNIDENTIFIED COMPOUNDS
ALKANES
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumpttve evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:15
Ending:
R-qc indicates t~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value.is known to be less than value given. L-actuat value is known to be greater than value g~iv LI-material was analyzed for bu. t not detected. the number 1s the minimum q~an n l1m1t
C-c-d bY_fllll" w-vahiliiport'iiililil chlo-consu 2 .,ents-ta tech.,lordliiiiil liiiiiil iiiiliiil 11:ii 1iii1! liiiiiil
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12464 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC003SL
Media: SOIL
RESULTS
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
1100U
440U
440U
440U
440U
440U
440U
1100U
440U
1100U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
Case Number: 25633
D Number: MP72
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
Org Contractor: COMPU
RESULTS
440U
440U
440U
440U
440U
440U
440U
44Q_lJ
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
1100U
440U
1100U
1100U
1100U
1100U
440U
25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 18:30
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
lJGJl<G
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
IN DENO (1,2,3,CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual.value is known to be less than value given. L-actual value is known to be weater than vatu~ ~~iv LI-material w~s a~alyzed for but not detected. the number is the minimum q"Jla · · n limit.
R-qc indrca.tes t~--unusable. compound may or may not be present. resampllng and reanalysis t ssary for venficat1on.
C-co-d by.,,. w-val-port"liiiil chlo-consa __ 2 . .,entss;aaia techiiiitlordfiiiiil iiiii1 iiii lii:l:ii -· ;:z:a
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12465 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC004SL
Media: SOIL D Number: MP73
RESULTS UNITS ANALYTE
540UJ
540UJ
540UJ
540UJ
540UJ
540UJ
540UJ
540UJ_
540UJ
540UJ
540UJ
540UJ
540UJ
540UJ
540UJ
54DUJ
540UJ
1400UJ
540UJ
540UJ
540UJ
540UJ
540UJ
540UJ
1400UJ
540UJ
1400UJ
540UJ
540UJ
540UJ
540UJ
540UJ
540UJ
540UJ
540UJ
160J
130J
540UJ
UG/KG 1,3-DICHLOROBENZENE
UG/KG 1,4-DICHLOROBENZENE
UG/KG 1,2-DICHLOROBENZENE
UG/KG BIS(2-CHLOROETHYL) ETHER
UG/KG HEXACHLOROETHANE
UG/KG · BIS(2-CHLOROISOPROPYL) ETHER
UG/KG · N-NITROSODI-N-PROPYLAMINE
UG/KG NITROBENZENE
UG/KG HEXACHLOROBUTADIENE
UG/KG 2-METHYLNAPHTHALENE
UG/KG 1,2,4-TRICHLOROBENZENE
UG/KG NAPHTHALENE
UGIKG . 4-CHLOROANILINE
UG/KG BIS(2-CHLOROETHOXY)METHANE
UG/KG ISOPHORONE
UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP)
UG/KG 2-CHLORONAPHTHALENE
UG/KG 2-NITROANILINE
UG/KG ACENAPHTHYLENE
UG/KG ACENAPHTHENE
UG/KG DIMETHYL PHTHALATE
UG/KG DIBENZOFURAN
UG/KG 2,4-DINITROTOLUENE
UG/KG 2,6-DINITROTOLUENE
UG/KG 3-NITROANILINE
UG/KG 4-CHLOROPHENYL PHENYL ETHER
UG/KG 4-NITROANILINE
UG/KG FLUORENE
UG/KG DIETHYL PHTHALATE
UG/KG N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
UG/KG HEXACHLOROBENZENE (HCB)
UG/KG 4-BROMOPHENYL PHENYL ETHER
UG/KG PHENANTHRENE
UG/KG ANTHRACENE
UG/KG DI-N°BUTYLPHTHALATE
UG/KG FLUORANTHENE
UG/KG PYRENE
UG/KG BENZYL BUTYL PHTHALATE
EXCESSIVE HOLDING TIME
Org Contractor: COMPU
RESULTS
540UJ
68J
190J
540UJ
540UJ
280J
74J
540UJ
540UJ
540UJ
540UJ
540UJ
540UJ
540UJ
54DUJ
540UJ
540UJ
54DUJ
1400UJ
540UJ
1400UJ
1400UJ
14D0UJ
1400UJ
540UJ
39
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08113/97 17:45
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
IND.ENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value giEiv LI-material was analyzed for but not detected. the number is the minimum qu;Jln · limit.
R-qc indicates thaA. unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-co-dbylliiP.willilfval"llllport'1111chlolii8iconsliiiii' 2.'llllll'ents-ta~ tech_,lord-lail lllil iiiil iiiil -iiii
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12465 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC004SL
Media: SOIL
RESULTS
100JN
600J
UNITS
UG/KG
UG/KG
D Number: MP73
ANALYTE
BENZOPYRENE (NOT A)
1 UNIDENTIFIED COMPOUND
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:45
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv LI-material was analyzed for but not detected. the number is the minimum q;,,an · · n limit.
R-qc indicates t~a-unusable. compound may or may not be present. resampllng and reanalysis i sary for verification.
C-c-d byilfil1' .w. val-port'liiil chl-consliiit5 2 . .,ent ... ta tech-hlord-iiil liiil liii -liiil
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12466 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-.SALEM, NC
·Program: NSF Case Number: 25633
Id/Station: JC005SL
Media: SOIL
RESULTS
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
930UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
930UJ
370UJ
930UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MP74
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
EXCESSIVE HOLDING TIME
Org Contractor: COMPU
RESULTS
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
930UJ
370UJ
930UJ
930UJ
930UJ
930UJ
370UJ
11
A-average value. NA-not analyzed. NAl-interterences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:00
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
R-qc indicates t~:a unusable. compound may or may not be present. resampling and reanalysis is sary for verification.
K-actuat value is known to be less than value given. L-actual value is known to be greater than value gi.,material was analyzed for but not detected. the number 1s the m1n1mum qu;,,nl n hm1t
C-confirmed by ~.w. valu-porteiliiii chlo-ons= 2 .• ents-tab tech,.,lord-rm la m mz::I
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12466 FY 1997 Project: 97 -0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC005SL
Media: SOIL
RESULTS UNITS
1000J UG/KG
D Number: MP74
ANALYTE
1 UNIDENTIFIED COMPOUND
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13197 19:00
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number 1s the m1mmum qu;Jln limit
R-qc indicates Iha-unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-co-dbylii\iP'w'avaluliiiforteiiiiilchloililr'ons& 2.c.ents-a tech'ilii'lord-------
EXTRACTABLES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12467 FY 1997 Project: 97 -0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC006SL
Media: SOIL
RESULTS
510U
510U
510U
510U
510U
510U
510U
510U
510U
510U
510U
510U
510U
510U
510U
510U
510U
1300U
510U
510U
510U
510U
510U
510U
1300U
510U
1300U
510U
510U
510U
510U
510U
460J
510U
510U
1800
1400
510U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
Case Number: 25633
D Number: MP75
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
Org Contractor: COMPU
RESULTS
510U
610
1300
510U
510U
2800
1000
810
220J
870
510U
510U
510U
510U
510U
510U
510U
510U
1300U
510U
1300U
1300U
1300U
1300U
95J
36
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:00
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO{A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DiMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum qu;,,n · n limit.
R-qc indicates tha-unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-co-by 111" ·w'a valuliliill'orte-chlor-onst-2.c.ents -• ech...,lord'l!!!!!!!!!!I 1!!!!!9 1!111 m= == iiii -
EXTRACT ABLES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA
Sample 12467 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC006SL
Media: SOIL
RESULTS
300JN
200JN
300JN
100JN
100JN
100JN
1000JN
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MP75
ANALYTE
ANTHRACENEDIONE
BENZOFLUORENE
BENZANTHRACENONE (2 ISOMERS)
BENZONAPHTHOTHIOPHENE
NAPHTHACENEDIONE
BENZOFLUORANTHENE (NOT B OR K)
BENZOPYRENE (NOT A, 2 ISOMERS)
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:00
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value giv~-material was analyzed for but not detected. the number is the minimum qu;/ln · limit.
R-qc indicates t~a-unusable. compound may or may not be present. resampling and reanalysis if sary for verification.
C-~-d by iiliiP' .w .. val-portelllill chloila"ons'lliii' 2.'lilii'ents-ao tech ... 1lord-------
EXTRACT ABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12468 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC007SL
Media: SOIL
RESULTS
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
1000U
410U
64J
410U
47J
410U
410U
1000U
410U
1000U
100J
410U
410U
410U
410U
3200
200J
410U
7600
5900
410U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MP76
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER ·
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
Org Contractor: COMPU
RESULTS
410U
2300
4300
410U
410U
8000
3600
2900
760
3100
410U
410U
410U
410U
410U
410U
410U
410U
1000U
410U
1000U
1000U
1000U
1000U
690
20
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:30
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferenceS. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. l-actual value is known to be greater than value g~iv LI-material was analyzed for but not detected. the number is the minimum q":1/lan · · limit.
R-qc indicates thaA unusable. compound may or may not be present. resampling and reanalysis i. sary for verification.
C-~d byailiiiii;1.w-val'lllilport ... chic-cons-2.1111ents-ta techilili'lord-------
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12468 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC0O?SL
Media: SOIL
RESULTS
300JN
?00JN
SO0JN
200JN
2000JN
300JN
300JN
90JN
300JN
300JN
200JN
?OO0JN
BOOOJ
200JN
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
·uG/KG
UG/KG
UG/KG
ANALYTE
ACRIDINE
Case Number: 25633
D Number: MP76
METHYLANTHRACENE (2 ISOMERS)
CYCLOPENTAPHENANTHRENE
PHENYLNAPHTHALENE
ANTHRACENEDIONE
NAPHTHALIC ANHYDRIDE
CYCLOPENTAPHENANTHRENONE
METHYLPYRENE
BENZOFLUORENE (2 ISOMERS)
BENZANTHRACENONE (2 ISOMERS)
BENZONAPHTHOTHIOPHENE
BENZOPYRENE (NOT A, 3 ISOMERS)
4 UNIDENTIFIED COMPOUNDS
NAPHTHCENEDIONE
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:30
Ending:
A-average value. NA-not analyzed. NAt-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value giv~-material was analyzed for but not detected. the number is the minimum qu;J/ln · · limit.
R-qc indicates t~~-unusable. compound may or may not be present. resampling and reanalysis is sary for verification.
C-c-dbyiiliP'.w-valWport°llillchlo~ns-2 . .,.ents-ab tech'ililflord------
•
-
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12469 FY 1997 Project: 97-0328
EXTRACTABLE$ SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC00BSL
Media: SOIL
RESULTS
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
890U
350U
350U
350U
350U
350U
350U
890U
350U
890U
350U
350U
350U
350U
350U
350U
350U
350U
54J
50J
350U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
Case Number: 25633
D Number: MP77
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
Org Contractor: COMPU
RESULTS
350U
350U
42J
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
890U
350U
890U
890U
890U
890U
350U
7
A-average value. NA-not analyzed. NAJ-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:35
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
R-qc indicates th .. unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum q;flan · · n limit.
C-c-d bylliiliP'·1iiil' val-port-chi-con,.s 2 .• uent ... ta teciw.rhlor'allll -1!!!11 all l!!!!!!!!!!!!I I!!!!
EXTRACTABLES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA
Sample 12469 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC008SL
Media: SOIL D Number: MP77 Org Contractor: COMPU
RESULTS UNITS ANALYTE
400JN UG/KG NAPTHOCHRYSENE (2 ISOMERS)
Production Date: 10/15/97 09:00
Produced by: John McConney
Requestor: PAT DEROSA
Project Leader: DEROSA "
Beginning: 08/13/97 20:35
Ending:
A-average value. NA-not analyzed. NAl-interierences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is.non to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum qu~n · limit.
R-qc indicates tha unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-co-by w-valu..,orte-chlor-onst-2"c'llllllrnls -•b ech'11111ord'l!!!!!!II l!!!!!!!!!I l!!!!!I l!!!!!I l!!!!!!!I ==
EXTRACT ABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12470 FY 1997 Project: 97-0328
EXTRACTABLE$ SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC009SL
Media: SOIL
RESULTS
360U
360U
360U
360U
360U
360U
360U
360U
360U
360U
360U
360U
360U
360U
360U
360U
360U
910U
360U
360U
360U
360U
360U
360U
910U
360U
910U
360U
360U
360U
360U
360U
360U
360U
360U
360U
360U
360U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MP78
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
. 2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 21 :45
Ending:
Org Contractor: COMPU
RESULTS UNITS
360U UG/KG
360U UG/KG
360U UG/KG
360U UG/KG
360U UG/KG
360U UG/KG
360U UG/KG
360U UG/KG
360U UG/KG
360U UG/KG
360U UG/KG
360U UG/KG
360U UG/KG
360U UG/KG
360U UG/KG
360U UG/KG
360U UG/KG
360U UG/KG
910U UG/KG
360U UG/KG
910U UG/KG
910U UG/KG
910U UG/KG
910U UG/KG
360U UG/KG
9 %
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALA TE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
.2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value givE-material was analyzed for but not detected. the number is the minimum qu;ant' limit.
R-qc indicates thatAunusable. compound may or may not be present. resampling and reanalysis is sary for verification.
C-co-byliir.wraavalu..,orte-chlo,..,onst-2.c-ents-ab ech,..lord... ------
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 13655 FY 1997 Project: 97 -0328
EXTRACTABLES SCAN
. Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC010SL
Media: SOIL
RESULTS
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
1000U
420U
420U
420U
420U
420U
420U
1000U
420U
1000U
420U
420U
420U
420U
420U
420U
420U
420U
54J
45J
420U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
Case Number: 25633
D Number: MP65
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER .
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
Org Contractor: COMPU
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:20
Ending:
RESULTS UNITS ANALYTE
420U
420U
420U
420U
420UJ
420UJ
420UJ
420UJ
420UJ
420UJ
420U
420U
420U
420U
420U
420U
420U
420U
1000U
420U
1000U
1000U
1000U
1000U
420U
21
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A}ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value giv-U-material was.analyzed for but not detected. the number 1s the minimum q;J/lant limit
R-qc indicates !~:a unusable. compound may or may not be present. resampling and reanalysis is sary for verification.
C-c=d byllliiiiii7.w-o val-port'alili chi-con-s 2 .• uent.,tab tech-hlor,_ --;al ---
EXTRACT ABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 13655 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC01 0SL
Media: SOIL
RES UL TS UNITS
2000J UG/KG
D Number: MP65
ANALYTE
3 UNIDENTIFIED COMPOUNDS
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:20
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value i: k'to be less than value given. L-actual value is known to be greater than value g-iv U-material was analyzed for but not detected. the number is the minimum q;J/lan · limit.
R-qc indicates tha unusable. compound may or may not be present. resamp1ing and reanalysis i sary for verification.
C-c=d by .w. val .... port'lllllf chl,..cons .... 2._,ent5111atab tech-hlord-------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12455 FY 1997 Project: 97 -0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC011 SL MD Number: MP66
Media: SOIL
RESULTS
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
11 OOUJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
11 OOUJ
430UJ
1100UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
UNITS
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UG/KG
UGIKG
UGIKG
UGIKG
UG/KG
UG/KG
UGIKG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MP66
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINEIDIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
EXCESSIVE HOLDING TIME
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
1100UJ
430UJ
11 OOUJ
1100UJ
1100UJ
1100UJ
430UJ
23
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08113/97 16:25
Ending:
UNITS
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UG/KG
UGIKG
UG/KG
UG/KG
UGIKG
UG/KG
UGIKG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-ANDIOR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLOR0-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimaled value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value gll;iv U-material was analyzed for but not detected. the number is the minimum q~a · n limit.
R-qc indicates thA_ unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-c-db~·1illf'val-portM'chl-con-s 2 ... uenlllllfla tecra!fhlor.... ------
EXTRACTASLES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12456 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC012SL MD Number: MP67
Media: SOIL
RESULTS
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
1100U
460U
460U
460U
460U
460U
460U
1100U
460U
1100U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MP67
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:56
Ending:
RES UL TS UNITS ANALYTE
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
1100U
460U
1100U
1100U
1100U
1100U
460U
28
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
R-qc indicates t~-unusable. compound may or may not be present. resampling and reanalysis · ssary for verification.
K-actual value is known to be less than value given .. L-actual value is known to be greater than value g~iv. U-material was analyzed for but not detected. the number is the minimum qu";JI· · n limit.
C-coad by ilii""w-valu-porte .. chloiiiiiifons-2 .• ents-ta tech.,lord-------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12456 FY 1997 Project: 97 -0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC012SL MD Number: MP67
Media: SOIL D Number: MP67
RES UL TS UNITS ANALYTE .
500J UG/KG 1 UNIDENTIFIED COMPOUND
lnorg Contractor: CHEM
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:56
Ending:
A•average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. l-actual value is known to be greater than value giv--material was analyzed for but not detected. the number is the minimum q;,,anr limit.
R-qc indicates Iha.unusable. compound may or may not be present. resampling and reanalysis is sary for verification.
C-c=d by~.w-val'Mllport'lllil chl~conslillr 2 'lllt•nt51111tab techlli:il'lordi;a ------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Productio.n Date: 10/15/97 09:00
Sample 12444 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC013SL MD Number: MP54
Media: SOIL
RESULTS
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
1000U
420U
420U
420U
420U
420U
420U
1000U
420U
1000U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG.
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MP54
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITR.OSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
• N-NITROSODIPHENYLAMI NE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALA TE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
1000U
420U
1000U
1000U
1000U
1000U
420U
21
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :50
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
R-qc indicates Iha unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-actual value i:iikn n lo be less than value given. L-actual value is known to be greater than value g-iv U-material was analyzed for but not detected. the number is the minimum q;Jlan · limit.
C-c='d by . ...., val-port ... chl.,..consa.s 2 . ....,ent ... tab tech-hlord-------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12444 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC013SL
Media: SOIL
RESULTS UNITS
400JN UG/KG
1000J UG/KG
Case Number: 25633
MD Number: MP54
D Number: MP54
ANALYTE
CARBOXYLIC ACID
2 UNIDENTIFIED COMPOUNDS
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John McConney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :50
Ending:
R-qc indicates Iha-unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g-iv U-material was analyzed for but not detected. the number is the minimum q;l/lan · · n limit.
C-c-d byflffl/l/1 ·"ilif val-port'lia' chl-con,.s 2.-•;ent'lllllta ·' tech-hlord-------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12445 FY 1997 Project: 97 -0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC014SL MD Number: MP55
Media: SOIL
RESULTS
400U
400U
400U
400U
400U
400U
400U
400U
400U
400U
400U
400U
400U
400U
400U
400U
400U
1000U
400U
44J
400U
400U
400U
400U
1DOOU
400U
1000U
65J
400U
400U
400U
400U
1700
11 OJ
400U
5400
2900
400U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MP55
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
D1-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
400U
1200
2300
400U
400U
4300
1800
940
270J
860
400U
400U
400U
400U
400U
400U
400U
400U
1000U
400U
1000U
1000U
1000U
1000U
390J
17
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 15:45
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
D1-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
R-qc indicates thA_ unusable. compound may or may not be present. resampling and reanalysis · ssary for verification.
K-actual value is known to be less than value given. L-actuar value is known to be greater than value g~i U-material was analyzed for but not detected. the number is the minimum q~a · · n limit.
C-c-dbyiilii'7.w-val'llllport-chl .. con511115 2._,entWllfta tech-hlord-------
EXTRACT ABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12445 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC014SL MD Number: MP55
Media: SOIL
RESULTS
90JN
500JN
700JN
100JN
100JN
100JN
300JN
100JN
200JN
2000JN
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
ACRIDINE
D Number: MP55
METHYLANTHRACENE (3 ISOMERS)
ANTHRACENEDIONE
NAPHTHALIC ANHYDRIDE
CYCLOPENTAPHENANTHRENONE
BENZOFLUORENE
BENZANTHRACENONE (3 ISOMERS)
BENZONAPHTHOTHIOPHENE
BENZOFLUORANTHENE (NOT B OR K)
BENZOPYRENE (NOT A, 2 ISOMERS)
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 15:45
Ending:
R-qc indicates th-unusable. compound may or may not be present. resamp1ing and reanalysis· ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~i U-material was analyzed for but not detected. the number is the minimum q~a · · n limit.
C-c-d byi/lll/r1 .w. val-port-chl'iillconslllr 2 . .,ent ... ta techilii'lord-------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12442 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC001 SW
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
Case Number: 25633
MD Number: MP52
D Number: MP52
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALA TE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :00
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actua. I value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum·q;,,an · · n limit.
R-qc indicates I~-unusable. compound may or may not be present. resampling and reanalysis i• ssary for verification.
C-co-dby,.,.w.valuiiliporteiliiichlo-consw 2 .• ents-ta tech.,lord-------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12443 FY 1997 Project 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC001 SD
Media: SEDIM
RESULTS
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
1400U
560U
560U
560U
560U
560U
560U
1400U
560U
1400U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MP53
D Number: MP53
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
1400U
560U
1400U
1400U
1400U
1400U
560U
41
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :30
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-materiat was analyzed for but not detected. the number is the minimum qu;Jln · · n limit.
R-qc indicates !~~unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-co-dby~.w-valuilillportelllillchlolll!tonslllt 2.'liil'ents-ab tech...,lord-------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12443 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC001 SD MD Number: MP53
Media: SEDIM
RESULTS UNITS
1000JN UG/KG
200JN UG/KG
3000J UG/KG
D Number: MP53
ANALYTE
PINENE (2 ISOMERS)
DIMETHOXYPROPENYLPHENOL
3 UNIDENTIFIED COMPOUNDS
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :30
Ending:
R-qc indicates tha-unusable. compound may or may not be present. resampling and reanalysis is sary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value giv~-material was analyzed for but not detected. the number is the minimum qu;Jln · limit.
C-co-dby_,,w.valu-orte-chlor-onst-2c-ents-ab ech~lord... ------
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12447 FY 1997 Project: 97-0328
EXTRACTABLE$ SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC002SW MD Number: MP57
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: MP57
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:45
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~·v U-material was analyzed for but not detected. the number 1s the minimum qu;Jln n limit
R-qc indicates t~~ unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-co-d by~ .w. valuiilliportelllii chlo-cons-2 .• entsililla tech'illltlord-------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12446 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC002SD MD Number: MP56
Media: SEDIM
RESULTS
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
1300U
500U
500U
500U
500U
500U
500U
1300U
500U
1300U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
UNITS
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
D Number: MP56
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTl-tALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
1300U
500U
1300U
1300U
1300U
1300U
500U
35
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08113197 12:30
Ending:
UNITS
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALA TE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2~CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv LI-material was analyzed for but not detected. the number is the minimum qu71· · n limit.
R-qc indicates t~--unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-confirmedby_.,.w.valuiiiporteiliichlo-ons-2 .• ents-a tech,.,lord------iiiil
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12446 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC002SD
Media: SEDIM
RES UL TS UNITS
400JN UG/KG
Case Number: 25633
MD Number: MP56
D Number: MP56
ANALYTE
CARBOXYLIC ACID
I norg Contractor: CH EM
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 12:30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is-n n to be less than value given. L-actuat value is known to be greater than value g~·v U-material was analyzed for but not detected. the number is the minimum qu;;/ln · limit.
R-qc indicates th unusable. compound may or may not be present. resampling and reanalysis i, ssary for verification.
C-c-d by w-val'laaport'9111 chlo..,,ons~ 2.'lilllii'ents-a tech,...,lord----all j;;;a
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12448 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC003SD MD Number: MP58
Media: SEDIM
RESULTS
470U
470U
470U
470U
470U
470U.
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
1200U
470U
470U
470U
470U
470U
470U
1200U
470U
1200U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MP58
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
1200U
470U
1200U
1200U
1200U
1200U
470U
31
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John McConney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :15
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE ·
% MOISTURE
R-qc indicates th unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-actual value;jjis kn n to be less than value given. L-actual value is known to be greater than value g-iv Li-material was analyzed for but not detected. the number is the minimum=-uan · limit.
C--edb ._ov"iilil"epor .. ech..,co'llats 2-tuen-etab fte"ll!llchlo-------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12448 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC003SD
Media: SEDIM
RESULTS
300JN
1000J
UNITS
UG/KG
UG/KG
Case Number: 25633
MD Number: MP58
D Number: MP58
ANALYTE
CARBOXYLIC ACID
ALKANES
lnorg Contractor: CHEM
Org Contractor: COM PU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11: 15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~ive. LI-material was analyzed for but not detected. the number 1s the minimum qu";Jlnt n hmil
R-qc indicates t~-unusable. compound may or may not be present. resampling and reanalysis i. ssary for verification.
C-confirmed by fl'' .w. valuiiiporteiili chlo.(ons-2 .• ents-ta tech-lord---iiiii liiiliiiil =m
EXTRACTABLES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12449 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC004SW MD Number: MP59
Media: SURFACEWA D Number: MP59
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UG/L
UG/L
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UGIL
UG/L
. UG/L
UGIL
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UGIL
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINEIDIPHENYLAMINE ·
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08113197 10:05
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UG/L
UG/L
UG/L
UGIL
UG/L
UG/L
UG/L
UG/L
UGIL
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
R--qc indicate_s thA. unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~·v U-material was analyzed for but not detected. the number is the minimum;;;Jlua · · n limit.
C--ed 'tllf1"' liilll"o v-repo'illlf e c~e co,.,ts -ituen.,eta f te'iiiiiiil chloliililll ll:::il l!!!!I I!!!! ---
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12450 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC004SD
Media: SEDIM
RESULTS
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
1400U
550U
550U
550U
550U
550U
550U
1400U
550U
1400U
550U
550U
550U
550U
550U
550U
550U
550U
87J
63J
550U
UNITS
UG/KG
UG/KG
UG/KG
U'3/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MP60
D Number: MP60
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER .
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COM PU
RESULTS
550U
550U
550U
550U
550U
87J
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
1400U
550U
1400U
1400U
1400U
1400U
550U
41
Produced by: John McConney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 10:30
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual.value is known to be less than value given. L-actual value is known to be weater than valu~ g~i LI-material w~s a~alyzed for but not detected. the number is the minimum ;;aua · n limit.
R-qc indicates th-unusable. compound may or may not be present. resamplmg and reanalysis ssary for venficat1on.
C--ed brlllll'1 -o va-epo-e ch., co,.,ts 2-tuen ... eta f tec-chlo----.---
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12450 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC004SD MD Number: MP60
Media: SEDIM
RESULTS
300JN
3000J
3000J
UNITS
UG/KG
UG/KG
UG/KG
D Number: MP60
ANALYTE
CARBOXYLIC ACID
ALKANES
2 UNIDENTIFIED COMPOUNDS
lnorg Contractor: CHEM
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 10:30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g-~iv. U-material was analyzed for but not detected. the number 1s the minimum qu";Jlnl n l1m1t
R-qc indicates t~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-co-dby,.,,.w.valwport-chloililll°ons-2 .• enls-ta tech.,lord-------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12451 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC005SW MD Number: MP61
Media: SURFACEWA
RESULTS
1DU
1DU
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
1DU
25U
10U
1DU
10U
10U
1DU
10U
25U
10U
25U
10U
10U
10U
10U
1DU
10U
10U
10U
1DU
10U
1DU
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: MP6 f
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE (HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 12:05
Ending:
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
1DU UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U -UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
25U UG/L
25U UG/L
25U UG/L
10U UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAJ-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g-iv U-material was analyzed for but not detected. the number is the minimum 3uan · limit.
R-qc indicates thaa unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C--edb...-,i .• ova-epo"lllllech...,co,...ts 2111111uen-eta ftec-chlor-11111 -----
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12452 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC005SD
Media: SEDIM
RESULTS
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
1200U
500U
500U
500U
500U
500U
500U
1200U
500U
1200U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG ·
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MP62
D Number: MP62
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE (HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
I norg Contractor: CH EM
Org Contractor: COMPU
RESULTS
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
1200U
500U
1200U
1200U
1200U
1200U
500U
35
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 12:35
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYREN E
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
R-qc indicates_!~~ unusable. compound may or may not be present. resampling and reanalysis I sary for verif1cat1on.
K-actual_value is known to be less than value given. L-actual value is known to be weater than valu~ ~~iv U-material w~~ a~alyzed for but not detected. the number is the minimum q:,,an · · limit.
C--edblilial" .• ova-epo'Willlechl-con-ts 2iiliiituent-eta ftec'llll'hlor.. ------
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12452 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Stalion: JC005SD
Media: SEDIM
RESULTS
600J
700J
UNITS
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MP62
D Number: MP62
1 UNIDENTIFIED COMPOUND
ALKANES
lnorg Contractor: CHEM
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 12:35
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value .. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-aclual value is known to be greater than value g~i U-material was analyzed for but not detected. the number 1s the minimum q;,,a n limit
R-qc indicates th-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C--ed bli9'1 -o va-epo-e chi-con-ts 2-tuent-eta f tec~htor-------
EXTRACT ABLES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12422 FY 1997 Project: 97-0328
EXTRACTABLE$ SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC006SW MD Number: MH94
Media: SURFACEWA D Number: MH94
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John McConney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 12:25
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALA TE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
R--qc indicates th unusable. compound may or may not be present. resampling and reanalysis ssary for verification.
K-actual value is kn wn to be less than value given. L-actual value is known to be greater than value g~i U-material was analyzed for but not detected. the number is the minimum:,,ua · n limit.
C--'11ed " 1-no v-repoilill'e c~e co'lilrts 11!11Wituerilll'eta of te~ chlo------1,91
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12423 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC106SW MD Number: MH95
Media: SURFACEWA D Number: MH95
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
1DU
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 12:30
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value i-~n wn to be less than value given. L-actual value is known to be greater than value g~·v LI-material was analyzed for but not detected. the number is the minimum q"31an · limit.
R-qc indicates th unusable. compound may or may not be present. resampling and reanalysis i ssary for verification. ·
C-c-d by" .w_ val'lliilliport1a chl°Mcons_. 2.r...,ents-ta~ tech~lord-----, , -. ' -
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12424 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC006SD MD Number: MH96
Media: SEDIM
RESULTS
1400U
1400U
1400U
1400U
1400U
1400U
1400U
1400U
1400U
1400U
1400U
1400U
1400U
1400U
1400U
1400U
1400U
3400U
1400U
1400U
1400U
1400U
1400U
1400U
3400U
1400U
3400U
1400U
1400U
1400U
1400U
1400U
1400U
1400U
1400U
230J
160J
1400U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MH96
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE •
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
1400U
1400U
180J
1400U
1400U
210J
1400U
1400U
1400U
1400U
1400U
1400U
150J
1400U
1400U
1400U
1400U
1400U
3400U
1400U
3400U
3400U
3400U
3400U
1400U
76
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 13:00
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUDRANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO{A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~ive. U-material was analyzed for but not detected. the number 1s the mrrnmum q;J/lant1 limit
R-qc indicates t~~ unusable. compound may or may not be present. resampling and reanalysis L sary for verification.
C-confirmed by., .w. valu-porteililii chlo-cons-2 .• ents-ta techwlord------
' . -
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12424 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC006SD MD Number: MH96
Media: SEDIM
RESULTS
2000JN
3000J
UNITS
UG/KG
UG/KG
D Number: MH96
ANALYTE
CARBOXYLIC ACID
1 UNIDENTIFIED COMPOUND
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 13:00
Ending:
R-qc indicates th unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-actual value is.n wn to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum qu;Jlnt" limit.
C-co-dby .w.val1'(f'ortelilllchloi'llr'ons-2 ..... ents-a tech .... lord-------
EXTRACT ABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA ProdL1_ction Date: 10/15/97 09:00
Sample 12434 FY 1997 Project: 97-0328
EXTRACTABLE$ SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC00?SW MD Number: MK09
Media: SURFACEWA D Number: MK09
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:26
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE .
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is.n n to be less than value given. L-actual value is known to be greater than value gll;i LI-material was analyzed for but not detected. the number is the minimum qu~n · limit.
R--qc indicates th unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-c-d by .w. val-port-chlo-cons-2."allt'ents-ta tech111f11ord------
, ' -
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12436 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC107SW MD Number: MK11
Media: SURFACEWA D Number: MK11
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:26
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAJ-illterferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is-non to be less than value given. L-actual value is known lo be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum qu;lln · limit.
R-qc indicates tha unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-co-dby .w.valu..,orte-chlo...,onsWIII 2.c.ents-ab ech,_lord-------
EXTRACTABLES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12435 FY 1997 Project: 97-0328
EXTRACTABLE$ SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC007SD MD Number: MK10
Media: SEDIM
RESULTS
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
. 1000U
1000U
1000U
1000U
2500U
1000U
1000U
1000U
1000U
1000U
1000U
2500U
1000U
2500U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
UNITS
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UG/KG
UGIKG
UG/KG
UGIKG
UGIKG
UGIKG
UG/KG
UG/KG
UGIKG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
D Number: MK10
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINEIDIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
1000U
1000U
1000U
. 1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
2500U
1000U
2500U
2500U
2500U
2500U
1000U
67
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:55
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value giv.U-material was analyzed for but not detected. the number is the minimum qu;,,nti · limit.
R-qc indicates !~~-unusable. compound may or may not be present. resampling and reanalysis is sary for verification.
C-confirmed by -.whllllllll value is reported see chlor-onst-2.c.ents -•b ech-lord... -----~ -
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12435 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC007SD
Media: SEDIM
RESULTS
1000JN
10000J
UNITS
UG/KG
UG/KG
Case Number: 25633
MD Number: MK10
D Number: MK10
ANALYTE
CARBOXYLIC ACID
5 UNIDENTIFIED COMPOUNDS
lnorg Contractor: CHEM
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:55
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value giv~-material was analyzed for.but not detected. the number is the minimum qu;,,nti limit.
R-qc indicates Iha.unusable. compound may or may not be present. resampling and reanalysis is sary for verification.
C-c-dbyial'.wiliilvalullillf'ortelllllllchlo-cons-2.~ents-ab tech..,lord-------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12438 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC00BSW MD Number: MK13
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: MK13
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N;PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 19:25
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value givE-material was analyzed for but not detected. the number is the minimum qu;J/lnt' limit.
R-qc indicates thatA,.inusable. com~ound may or may not be presen_t. resampling_~nd reanalysis is sary for verification.
C-c~by..,.w.valu-porte-chlo_,ons-2.~ents-ab techra.ilord------, ' -
EXTRACTABLES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12437 FY 1997 Project: 97-0328
EXTRACTABLE$ SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC008SD
Media: SEDIM
RESULTS UNITS
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
1200U
500U
500U
500U
500U
500U
500U
1200U
500U
1200U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MK12
D Number: MK12
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALA TE
lnorg Contractor: CHEM
Org Contractor: COM PU
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
RES UL TS UNITS ANALYTE
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
1200U
500U
1200U
1200U
1200U
1200U
500U
34
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
BIS(2-ETHYLHEXYL) PHTHALA TE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
R-qc indicates Iha-unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-actua. I value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum qu;,,nt" · limit.
C-co.dbyi9J'.w'lililivaluililit"ortellllchlo-ons-2.c.ents-a tech'81111lord-------
EXTRACTABLES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12437 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC00BSD MD Number: MK12
Media: SEDIM
RESULTS UNITS
500JN UG/KG
D Number: MK12
ANALYTE
CARBOXYLIC ACID
lnorg Contractor: CHEM
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
A-average value. NA-not analyzed. NAJ-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv LI-material was analyzed for but not detected. the number 1s the minimum qu~nt hmit
R-qc indicates Iha-unusable. compound may or may not be present. resampling and reanalysis i sary for verification. ·
C-c~-d by ill" w-valu-orte-chlo.,ons-2.c.ents -a ech'ililflord-------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12439 FY 1997 Project: 97-0328
EXTRACTABLE$ SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC 1 OSSO
Media: SEDIM
RESULTS
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
1200U
490U
490U
490U
490U
490U
490U
1200U
490U
1200U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MK14
D Number: MK14
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
•N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
1200U
490U
1200U
1200U
1200U
1200U
490U
33
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALA TE
BENZO(A)ANTHRACENE
CHRYSENE
·3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interierences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less. than value given. L-actual value is known to be greater than value g-iv U-material was analyzed for but not detected. the number is the minimum qu;,,nt' limit.
R-qc indicates that_A,unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-c-dby .. w-val,.port"lllllchlo-cons-2.~rents-tab tech ... lord-------
EXTRACT ABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12439 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC 1 0SSD
Media: SEDIM
RES UL TS UNITS
400JN UG/KG
Case Number: 25633
MD Number: MK14
D Number: MK14
ANALYTE
CARBOXYLIC ACID
lnorg Contractor: CHEM
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum qu;,,nti limit.
R-qc indicates that.A1nusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-co.d by llll'wifllii valullllllr'orte-chlo_,onslllf 2 ._ents-ab tech._lord-----. -..
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12441 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC009SW MD Number: MP51
Media: SURFACEWA D Number: MP51
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE .
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:45
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL0 4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-aVerage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual_value is known to be less than value given. L-actual value ls known to be weater than valu? ~-iv U-material w~7 a~atyzed for but not detected. the number is the minimum q;;;/lanr limit.
R.qc indicates thatAnusable. compound may or may not be present. resampllng and reanalysis I sary for venf1cat1on. -
C--ed b....., .• o val .. port_. chi-con~ts 2-uenl_,lab f teci_,hlor-------
EXTRACT ABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12440 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC009SD MD Number: MP50
Media: SEDIM
RESULTS
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
1700U
670U
670U
670U
670U
670U
670U
1700U
670U
1700U
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MP50
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADI_ENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE ·
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
670U
1700U
670U
1700U
1700U
1700U
1700U
670U
51
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/9716:30
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-rnaterial was analyzed for but not detected. the number is the minimum q3an · limit.
R-qc indicates Iha.unusable. compound may or may not be present. resampling and reanalysis i ssary for verification. .
C-r-edb__.. .• ova-epo,...echl-con .. ts 211111tuen-eta ftec_,hlor-------
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12440 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC009SD MD Number: MP50
Media: SEDIM
RESULTS
900JN
2000J
UNITS
UG/KG
UG/KG
D Number: MP50
ANALYTE
CARBOXYLIC ACID
ALKANES
lnorg Contractor: CHEM
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/9716:30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number 1s the minimum qu~nt limit
R-qc indicates !~~unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-co-d by _,.w. valuilili'orte-chlor-onst-2.c.ents -• ech'Wlord'IIIII ------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12453 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC01 0SW
Media: SURFACEWA
Case Number: 25633
MD Number: MP63
D Number: MP63
RESULTS
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
25UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
25UJ
10UJ
25UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
.HEXACHLOROBENZENE (HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26, 1984)
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
25UJ
10UJ
25UJ
25UJ
25UJ
25UJ
10UJ
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 09:40
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum q=-an · limit.
R-qc indicates Iha.unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-c-ed blliiillP .• o va-epo"Me chi-conllillllls 2-tueni_.ta f tecllllfhlor-------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12454 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC010SD MD Number: MP64
Media: SEDIM
RESULTS
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
1100U
430U
430U
430U
430U
430U
430U
1100U
430U
1100U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG.
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MP64
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
1100U
430U
1100U
1100U
1100U
1100U
430U
24
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 09:25
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
· A-average value. NA-not analyzed. NAt-interferences. J-eslimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known lo be greater than value g-iv · LI-material was analyzed for but not detected. the number is the minimum q;;,,ant' limit.
R-qc indicates thaAunusable. compound may or may not be present. resampling and reanalysis i sary for verification. C--ed b.., .... o valllafportllal' chi ... con-ts 2S111fuenl..,tab tec~hlonlm ------
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12429 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC011 SW MD Number: MJ01
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
1DU
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: MJ01
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COM PU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:25
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum q~an · limit.
R-qc indicates thatAunusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-cadby .... w.valL-port'lillfchl-con5111W 2 . ..,ent._ta _ tech-hlord-------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12430 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC011 SD MD Number: MJ02
Media: SEDIM
RESULTS
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
1200U
500U
500U
500U
500U
500U
500U
1200U
500U
1200U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
UNITS
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UGIKG
UGIKG
UG/KG
UG/KG
UGIKG
UGIKG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UGIKG
UGIKG
D Number: MJ02
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2;4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINEIDIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
1200U
500U
1200U
1200U
1200U
1200U
500U
34
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08112197 18:45
Ending:
UNITS
UG/KG
UG/KG
UGIKG
UGIKG
UG/KG
UGIKG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual_value is known to be less than value given. L-actual value is known to be weater than valu~ ~~iv. U-material w~s a~alyzed for but not detected. the number is the minimum q;J/lan · · n limit.
R-qc indicates ,!~-unusable. compound may or may not be present. resampllng and reanalysis I ssary for venficat1on.
C-c-ed by.....,.wlllllo val-eport'iilair chi-con-s 2 .• uentllill'ta tecr-hlor'IIII ------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12430 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC011 SD MD Number: MJ02
Media: SEDIM
RESULTS UNITS
400JN UG/KG
D Number: MJ02
ANALYTE
CARBOXYLIC ACID
lnorg Contractor: CHEM
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value .is kn wn to be Jess than value given. L-actual value is known to be greater than value 911.;· LI-material was analyzed for but not detected. the number is the minimum q';lla n limit.
R-qc indicates th unuSable. compound may or may not be present. resampling and reanalysis ssary for verification.
C-c-d b~ .w. valtillllfport11111 chl .. conslilllf 2.'lll'ent51111ta . tech-hlord------
' 11111!
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12420 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC012SW
Media: SURFACEWA
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
Case Number: 25633
MD Number: MH92
D Number: MH92
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE (HCB)
4-BROMOPHENYL PHENYLETHER
PHENANTHRENE
ANTHRACENE
Dl-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAJ-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/9711:12
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
Dl-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
R-qc indicates Iha unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value i;ikn n to be less than value given. L-actual value is kno_wn to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum qu;,,n · limit.
C-c'iillld by _w_ val'lillport'IIIII chl~cons-2.'lla'ents-ta tech11111f11ord-------
' '
EXTRACT ABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12421 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC012SD MD Number: MH93
Media: SEDIM
RESULTS
490U
490U
490U
490U
490U
490U
490U
4900
490U
490U
490U
490U
490U
490U
490U
490U
490U
1200U
490U
490U
490U
490U
490U
490U
1200U
490U
1200U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MH93
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE .
BENZYLBUTYLPHTHALATE
I norg Contractor: CH EM
Org Contractor: COMPU
RESULTS
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
1200U
490U
1200U
1200U
1200U
1200U
490U
33
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John McConney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 11 :30
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLOR0-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
R-qc indicates"t~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification. .
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv Li-material was analyzed for but not detected. the number 1s the minimum q;J/lan n limit
C-" ed b__..v.o val-portlillllr chi-con-ls 2-uentm"la . f teci-.,hlor,... ----IBII -
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12421 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC012SD
Media: SEDIM
RESULTS
200JN
600J
UNITS
UG/KG
UG/KG
ANALYTE
PINENE
Case Number: 25633
MD Number: MH93
D Number: MH93
1 UNIDENTIFIED COMPOUND
lnorg Contractor: CHEM
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 11 :30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value giltiv LI-material was analyzed for but not detected. the number is the minimum qu;Jln · limit.
R-qc indicates !~a-unusable. compound may or may not be present. resampting and reanalysis i ssary for verification.
C-co-dby ..... w.val-port .... chlo.,ons-2 . .,.ents-a tech...,lord-------
EXTRACTABLES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12431 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC013SW
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
Case Number: 25633
MD Number: MK06
D Number: MK06
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHAL}\TE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:35
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is~n n to be less than value given. L-actual value is known to be greater than value g~i U-material was analyzed for but not detected. the number is the minimum qu~n · limit.
R-qc indicates tha unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C:c-dby .w.valu_,orte-chlo_,ons-2.c .. ents-a tech....,lord--------.
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12432 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC013SD
Media: SEDIM
RESULTS
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
· 11 oou 4Sou·
450U
450U
450U
450U
450U
1100U
450U
1100U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MK07
D Number: MK0?
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
1100U
450U
1100U
1100U
1100U
1100U
450U
27
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:50
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALA TE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual_value is known to be less than value given. L-actual value is known to be ~realer than valu~ g~iv LI-material w~~ a~alyzed for but not detected. the number is the minimum qu;Jln · · n limit.
R-qc indicates t~a-unusable. compound may or may not be present. resamphng and reanalysis ssary for verif1cat1on.
C-co-dby..,..w.valu-orte-chlolilf'ons-2.c.ents-a tech'iaii'lord-1111 ---. ...
' -
EXTRACTABLES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA
Sample 12432 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC013SD MD Number: MK07
Media: SEDIM
RESULTS UNITS
300JN UG/KG
D Number: MK0?
ANALYTE
CARBOXYLIC ACID
lnorg Contractor: CHEM
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/9716:50
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum qu;Jln · limit.
R-qc indicates thaA unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-c-dby,.,..w.valullll1'ort'11111chlo_,onsiat 2~ents-ta tech,..,lord-------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12419 FY 1997 Project: 97-0328
EXTRACTABLE$ SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC014SW MD Number: MH91
Media: SURFACEWA D Number: MH91
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
1J
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
2J
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
1J
25U
25U
25U
2J
10U
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:45
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actua1 value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum q;,,an · · n limit.
R-qc indicates tha-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-c-d by,., .w.., val'liilport'1a chlolillcons-2 'IIMlfents-ta tech_,lord-------
EXTRACTABLES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12418 FY 1997 Project: 97 -0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC014SD MD Number: MH90
Media: SEDIM
RESULTS
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
1900U
740U
740U
740U
740U
740U
740U
1900U
740U
1900U
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
UNITS
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UG/KG
UG/KG
D Number: MH90
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
740U
1900U
740U
1900U
1900U
1900U
1900U
740U
56
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08112197 09:33
Ending:
UNITS
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-ANDIOR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv. U-material was analyzed for but not detected. the number is the minimum qu;Jln · · n limit.
R-qc indicates t~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-co.dby,.,.w.,valu-porte-chlo-consw 2 .• ents-ta tech,.,lord-------
EXTRACT ABLES. SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12418 FY 1997 Project: 97 -0328
MISCELLANEOUS COMPOUNOS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC014SD MD Number: MH90
Media: SEDIM
RES UL TS UNITS
3000J UG/KG
D Number: MH90
ANALYTE
3 UNIDENTIFIED COMPOUNDS
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:33
Ending:
R-qc indicates th unusable. compound may or may not be present. resampling and reanalysis· ssary for verification.
K-actual valueilfis k n to be less than value given. L-actual value is known to be greater than value g~i U-material was analyzed for but not detected. the number is the minimum q~a n limit.
C-c-d b 1.;a, val-port.., chl .... con ... s 2.-.,ent ... ta tech-hlord-------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12427 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC015SW MD Number: MH99
Media: SURFACEWA D Number: MH99
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALA TE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/9711:47
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
R-qc indicates thA_ unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value gll;i LI-material was analyzed for but not detected. the number is the minimum qu~n limit.
C-c-dby,,,,,...w.valu-porte-chlollal"ons-2c-ents-ta tech,..,lord-------
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12428 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC015SD
Media: SEDIM
Case Number: 25633
MD Number: MJOO
D Number: MJOO
RESULTS
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
1500U
600U
600U
600U
600U
600U
600U
1500U
600U
1500U
600U
600U
600U
600U
600U
310J
600U
600U
930
660
600U
UNITS ANAL YTE
UG/KG 1,3-DICHLOROBENZENE
UG/KG 1,4-DICHLOROBENZENE
UG/KG 1,2-DICHLOROBENZENE
UG/KG BIS(2-CHLOROETHYL) ETHER
UG/KG HEXACHLOROETHANE
UG/KG BIS(2-CHLOROISOPROPYL) ETHER
UG/KG N-NITROSODI-N-PROPYLAMINE
UG/KG NITROBENZENE
UG/KG HEXACHLOROBUTADIENE
UG/KG 2-METHYLNAPHTHALENE
UG/KG 1,2,4-TRICHLOROBENZENE
UG/KG NAPHTHALENE
UG/KG 4-CHLOROANILINE
UG/KG BIS(2-CHLOROETHOXY)METHANE
UG/KG ISOPHORONE
UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP)
UG/KG 2-CHLORONAPHTHALENE
UG/KG 2-NITROANILINE
UG/KG ACENAPHTHYLENE
UG/KG ACENAPHTHENE
UG/KG DIMETHYL PHTHALATE
UG/KG DIBENZOFURAN
UG/KG 2,4-DINITROTOLUENE
UG/KG 2,6-DINITROTOLUENE
UG/KG 3-NITROANILINE
UG/KG -4-CHLOROPHENYL PHENYL ETHER
UG/KG 4-NITROANILINE
UG/KG FLUORENE
UG/KG DIETHYL PHTHALATE
UG/KG N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
UG/KG HEXACHLOROBENZENE (HCB)
UG/KG 4-BROMOPHENYL PHENYL ETHER
UG/KG PHENANTHRENE
UG/KG ANTHRACENE
UG/KG DI-N-BUTYLPHTHALATE
UG/KG FLUORANTHENE
UG/KG PYRENE
UG/KG BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
600U
300J
600
600U
600U
1300J
490J
320J
600U
320J
600U
600U
600U
600U
600U
600U
600U
600U
1500U
600U
1500U
1500U
1500U
1500U
67J
45
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 12:15
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
0I-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLOR0-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
R-qc indicates Iha.unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~·v LI-material was analyzed for but not detected. the number is the minimum qu;Jln · · limit.
C-co-d by ial' w-valu-orte-chlo~ons-2.ca,ents -• tech'ilililord-------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12428 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC015SD
Media: SEDIM
RESULTS
300JN
200JN
600JN
UNITS
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MJ00
D Number: MJ00
CARBOXYLIC ACID
ANTHRACENEDIONE
BENZOFLUORANTHENE (NOT B OR K)
lnorg Contractor: CHEM
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John McConney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 12:15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g-iv U-material was analyzed for but not detected. the number is the minimum qu~n · limit.
R-qc indicates Iha.unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-c-dbyj9"w-valu.,orte-chlolllll"ons-2.~ents-a tech-1lord-------
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12433 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC016SD
Media: SEDIM
RESULTS
1100U
11D0U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
11D0U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
2700U
11D0U
11D0U
1100U
1100U
1100U
1100U
2700U
1100U
2700U
'1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
11 DOU'
1100U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MK0B
D Number: MK0B
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
1100U
1100U
1100U
1100U
1100U
1100U
11D0U
1100U
1100U
1100U
1100U
1100U
11D0U
1100U
1100U
1100U
1100U
1100U
2700U
1100U
2700U
2700U
2700U
2700U
1100U
69
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 15:35
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALA TE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
R-qc indicates tha' unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-actual value isano n to be less than value given. L-actual value is kno_ wn to be greater than value g~iv LI-material was analyzed for but not detected. the number is the minimum qu~n · limit.
C-c-dby w-valullil9'orte-chlo~ons-2,~ents-ab lech,...,lord-------
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12433 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC016SD MD Number: MK08
Media: SEDIM
RESULTS
900JN
4000J
6000J
UNITS
UG/KG
UG/KG
UG/KG
D Number: MK0S
ANALYTE
CARBOXYLIC ACID
ALKANES
3 UNIDENTIFIED COMPOUNDS
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAJ-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 15:35
Ending:
R-qc indicates th unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value ~is kn n to be less than value given. L-actual value is known to be greater than value g~· U-material was analyzed for but not detected. the number ts the minimum q"'a n ltmit
C-c-d by . .,. val._port'lllllf chl'allcon5M5 2 . ..,ent'afta tech-hlord-------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12425 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC017SW MD Number: MH97
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: MH97
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:30
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
R--qc indicates th .. unusable. compound may or may not be present. resampling and reanalysis · ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~i U-material was analyzed for but not detected. the number is the minimum q~a · · n limit.
C-c-dby_,,w.val-port"lllifchl-consw 2 .• ent"llillfta 'tech-hlord-------
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12426 FY 1997. Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC017SD MD Number: MH98
Media: SEDIM
RESULTS
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
1000U
410U
410U
410U
410U
410U
410U
1000U
410U
1000U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MH98
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITRO BENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
1000U
410U
1000U
1000U
1000U
1000U
410U
20
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:40
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value i~kn n to be less than value given. L-actual value is known to be greater than value g~i U-material was analyzed for but not detected. the number is the minimum q~a · n limit.
R-qc indicates th unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-c.,d by ·"11111' val._-port.., chic-con'lillls 2.-uent,_ta tec'11ahlor~ ------,. I
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12412 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC018SW MD Number: LL02
Media: SURFACEWA D Number: LL02
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE (HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
. lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 16:32
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
R-qc indicates thaA unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv Li-material was analyzed for but not detected. the number is the minimum q;,,an · · n limit.
C-c-d byrJa" .,., valwportw chl'llilll con-s 2 .• uent-ta tech-hlor'Wall -----' .
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12413 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC018SD MD Number: LL03
Media: SEDIM
RESULTS
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
2300UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
2300UJ
910UJ
2300UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: LL03
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
EXCESSIVE HOLDING TIME
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
91DUJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
.910UJ
2300UJ
910UJ
2300UJ
2300UJ
2300UJ
2300UJ
910UJ
64
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 17:35
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALA TE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value iakno n to be less than value given. L-actual value is known to be greater tha.n value g-iv U-material was analyzed for but not detected. the number 1s the mmrmum q";tlan lrmit
R-qc indicates tha unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-c,.db¥_ ·1ill'val·-port,..chlc1illcon,_s 2.c-Jent,--ta tech-hlord-------I .
EXTRACTABLES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12413 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC018SD MD Number: LL03
Media: SEDIM
RES UL TS UNITS
40000J UG/KG
1 0000J UG/KG
D Number: LL03
ANALYTE
10 UNIDENTIFIED COMPOUNDS
ALKANES
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-eslimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 17:35
Ending:
R-qc indicates th unusable. compound may or may not be present. resampting and reanalysis i ssary for verification.
K-actual value is~n n to be less than value given. L-actual value. is known to be greater than value ga;i U-material was analyzed for but not detected. the number is the minimum qu;an limit.
C-c-d by .w-val,...,ort .... chlo-cons-2.'ll!ll'ents-a tech..,lord----. ---
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12414 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC019SD MD Number: LL04
Media: SEDIM D Number: LL04
RESULTS UNITS
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
2000UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
2000UJ
780UJ
2000UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
120J
120J
780UJ
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
EXCESSIVE HOLDING TIME
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
2000UJ
780UJ
2000UJ
2000UJ
2000UJ
2000UJ
780UJ
58
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 17:50
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG.
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
R-qc indicates thaA. unusable. compound may or may not be present. resampling an_d reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv LI-material was analyzed for but not detected. the number 1s the m1rnmum q~an n 1tm1t
C-c-dby_,,w.val-port ... chl-cons-2-ents-ta tech-lordilll ----, --
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12415 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC020SW
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
· 10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
Case Number: 25633
MD Number: LL05
D Number:·LL05
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE ·
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 15:00
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actuat value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum q;J/lan · n limit.
R-qc indicates thaAunusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-c-dby ..... w .. val'lillport1illlchlo-cons .. 2-ient'1ata techmt'lord------
' ' -
EXTRACT ABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12416 FY 1997 Project: 97-0328
EXTRACTABLE$ SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC021 SW
Media: SURFACEWA
RESULTS
10U.
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
Case Number: 25633
MO Number: LL06
D Number: LL06
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
0I-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 17:00
Ending:
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
25U UG/L
25U UG/L
25U UG/L
10U UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
0I-N-OCTYLPHTHALA TE
BENZO(B ANO/OR K)FLUORANTHENE
BENZO-A-PYRENE
IN DENO (1 ;2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLOR0-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value i~kn n to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum q;J/lan · limit.
R-qc indicates Iha· unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-c--d by .w_ val~port'IIIII chlo-cons.., 2 ,..,ent511111tali tech...,lord----.. --
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12417 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC021SD MD Number: MH89
Media: SEDIM
RESULTS
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
2000U
BOOU soou
BOOU
BOOU
BOOU
BOOU
2000U
BOOU
2000U
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MH89
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
BOOU soou soou
BOOU
BOOU soou
BOOU
BOOU
BOOU
BOOU soou
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
BOOU
2000U
BOOU
2000U
2000U
2000U
2000U
BOOU
59
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 18:40
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value isano n to be less than value given. L-actual value is known to be greater than value_ g-iv U-material was analyzed for but not detected. the number is the minimum qu";Jln · limit.
R-qc indicates tha' unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-c-d by ,. .w. valumport"m chlomcons ... 2.1111:fentsi::mtab tech..,tord91!1 1!!!!!!1!!!! l!!!!!!l!!I 1!!!111 l!!!!!!I -, __
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12417 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC021 SD MD Number: MH89
Media: SEDIM D Number: MH89
RES UL TS UNITS ANALYTE
900J UG/KG 1 UNIDENTIFIED COMPOUND
lnorg Contractor: CHEM
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 18:40
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptlve evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number 1s the minimum qu;Jln n limit.
R-qc indicates t~~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification. _
C-c.,d by~ .w. val-port'1ai chlo(ilfons-2 .• ents-ta . techillil"lordlllil ------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12457 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC001 PW
Media: GROUNDWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
Case Number: 25633
MD Number: MP68
D Number: MP68
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20: 15
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
Dl-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
R-qc indicates _t~~-unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-actual value ls known to be less than value given. L-actual value is known to be greater than value g~iv LI-material was analyzed for but not detected. the number 1s the m1n1mum q;Jlan l1m1t
C-c-ed by_. .• o val-portilir chl-~on-s 2 .• uents1111111eta of technical chlord. ------
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97·09:00
Sample 12458 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC002PW MD Number: MP69
Media: GROUNDWA
RESULTS
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
25UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
25UJ
10UJ
25UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: MP69
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26,1984)
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
25UJ
10UJ
25UJ
25UJ
25UJ
25UJ
10UJ
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 21 :00
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALA TE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO{A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is~n n to be less tha. n value given. L-actual value is known to be greater than value gEiV. U-material was analyzed for but not detected. the number is the minimum qu;i, limit.
R-qc indicates Iha unusable. compound may or may not be present. resamp!ing and reanalysis i sary for verification. ---
C-c-d by · .wllllll val~porte-chloa.cons-2.~ents-ab tech1-1lord---
' ' -
J
It
I
I
MEMORANDUM
I Date: 12/11 /97
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I Subject: Results of METALS INORGANIC Sample Analysis
97-0329 JOHNSON CONTROLS GLOBE
RECEf\11=o
DE:c 19 1997
SUPERFUND SECTION I
I
I ,
WINSTON-SALEM, NC
From: Keith Bates ;::.~
To: PAT DEROSA
Thru: QA Office
Please substitute the lead results for those reported September 16, 1997. The original laboratory, Antee Ltd.,
f eanalyzed lead by graphite furnace due to suspected ICP interference. All other metal results remain the same
s those previously reported.
The Region IV, Science and Ecosystem Support Division reanalyzed the samples for all metals. Those results,
■eported on November 26, 1997, should be used for decision purposes.
11 you have any questions, please contact me.
1•
1
ITTACHMENT
I
I
~
I
I
J
~
I
I
I
I
I
I
I ,
I
I
I
I
I
I
I
INORGANIC DATA REVIEW DOCUMENT
United States Environmental Protection Agency
Region IV
Environmental Services Division
980 College Station Road, Athens, GA 30613
Date: 11 December 1997
Subject: Review of Inorganic Contract Data
Case No. 25633 SAS No.
Contract Lab Name:--"An,.,_,t~e~c~h..._,L..,__..t~d~.-----------
Region IV Project No.: 97-0329
SMO Traffic Nos.: MDMP65. MDMP70-MDMP78
Reg. IV SAD Nos. :_.1~2~4~7w6~-~1~2~4"-'-7~5 ___________ _
Matrix types: Water __ Soil/Sect. _J,_Q_ Waste
Review performed by:_.,K~e~iut~h,_.B~a~t~e.,_.,_s ______________ _
Review Codes
A-Acceptable: All QC criteria met. No data qualified based on these
items.
P-Provisional: Some QC criteria were exceeded resulting in data
qualifiers being assigned based on these items.
U-Unacceptable: The QC criteria were exceeded to such an extent that
the associated data was rejected based on these items.
N/A-Not Applicable: This item does not apply to the case being
reviewed.
I. Sample Holding Times (Technical holding times; waters only)
Metals (6 mos.)
Mercury (28 days)
Cyanide (14 days)
NIA
NIA
NIA
Remarks: Soil samples only.
I
I
I
I
I
I
I ,
I
I
I
I
I
I
It
I
I
II. Calibration
Initial Calib.
Init. Cal. Ver.
Cont. Cal. Ver.
ICP Furnace
A
A
A
Mercury CN
Remarks: CRA ran at 2X CRDL instead of at the CRDL as required by
the functional guidelines, but all sample results are greater than
2X CRDL. The CCV was ran at the same concentration as the rev.
III. Blanks
IV.
V.
Calibration Blanks
Preparation Blanks
Blind Blanks
Remarks:
A
A
NIA
ICP Interference Check Sample
False Positives
False Negatives
Remarks:
NIA
NIA
Spiked Sample Results
Matrix Spike
Blind Spike
Water
NIA
NIA
Soil
A
NIA
Remarks: The lead matrix spike recovery was 3828%. The data is
not flagged because the sample concentration is greater than 4X
the spike concentration.
VI. Other QC
Matrix Duplicates A
LCS A
Serial Dilution Results NIA
Linear Range Check (2xCRDL) NIA
Remarks:
I
I
I
I
I
I ,
I
I
I
I
I
I
'It
I
I
VII. Deliverables
Cover Page NIA
Form I A
QC Summary Forms A
Raw Data
Traffic Reports
Digestion Logs
Preparation Logs
Run Logs
A
NIA
NIA
A
A
Remarks: Sample prepared for ICP analysis were used to run the
graphite furnace analysis.
VIII. Contact with Contract Lab required during data review?
Yes No_z_
Remarks:
-=T~ArN,_S
Sample 12476 FY 1997
METALS SCAN
--Project: 97-0329
THIS TEST SET IS INCOMPLETE
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
ld/Station:JB010SL MD Number: MP65 lnorg Contractor: ANTEC
Media: SOIL
RESULTS UNITS ANALYTE,
13000J MG/KG ALUMINUM
0,6UJ MG/KG ANTIMONY
0,96J MG/KG ARSENIC
100J MG/KG BARIUM
0,85J MG/KG BERYLLIUM
4,1JN MG/KG CADMIUM
1100J MG/KG CALCIUM
32J MG/KG CHROMIUM
18J MG/KG COBALT
20J MG/KG COPPER
19000J MG/KG IRON
34 MG/KG LEAD
2500J MG/KG MAGNESIUM
760J MG/KG MANGANESE
0,34J MG/KG TOTAL MERCURY 19J MG/KG NICKEL
2200J MG/KG POTASSIUM
0,32U MG/KG SELENIUM
2.6J MG/KG SILVER
54 MG/KG SODIUM
0.36UJ MG/KG THALLIUM
51J MG/KG VANADIUM
370J MG/KG ZINC
23 % %MOISTURE
- --Pr-ion-:. o~P
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:20
Ending:
A-average value. NA-not analyzed. NAl-interferences. J--estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R.qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
W 1,WA~_N.,,... __ s _________ -___ 11111\ __ -___ N 1'111D, ... EN~
Sample 12477 FY 1997 Project: 97-0329
METALS SCAN THIS TEST SET IS INCOMPLETE
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
ld/Station:JB001SL MD Number: MP70 lnorg Contractor: ANTEC
Media: SOIL
RESULTS UNITS ANALYTE
6200J MG/KG ALUMINUM
0.58UJ MG/KG ANTIMONY
1UJ MG/KG ARSENIC
53J MG/KG BARIUM
0.57J MG/KG BERYLLIUM
2.3J MG/KG CADMIUM
490J MG/KG CALCIUM
20J MG/KG CHROMIUM
9.BJ MG/KG COBALT
14J MG/KG COPPER
8700J MG/KG IRON
17 MG/KG LEAD
1600J MG/KG MAGNESIUM
210J MG/KG MANGANESE
O.0BUJ MG/KG TOTAL MERCURY
10J MG/KG NICKEL
1000J MG/KG POTASSIUM
0.31U MG/KG SELENIUM
2.3J MG/KG SILVER
46 MG/KG SODIUM
0.36U MG/KG THALLIUM
25J MG/KG VANADIUM
32J MG/KG ZINC
14 % % MOISTURE
---ProWl!ion -1r 09-
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumpt1ve evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis 1s necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
~--t:l~A~_N_.,.., __ s _____________ anti. ____ FIIIIJ __ N ._D,.EN~ --Prcll!llion -: 1f/'7 09 ..
Sample 12478 FY 1997 Project: 97-0329
METALS SCAN THIS TEST SETIS INCOMPLETE
Facilily: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
ld/Station:JB101SL MD Number: MP71 lnorg Contractor: ANTEC
Media: SOIL
RESULTS
6000J
0.64UJ
0.84J
65J
0.61J
2.2J
640J
19J
10J
15J
8400J
19
1600J
370J
0.12UJ
9.7J
1000J
0.34U
2.1J
38
0.39U
25J
30J
15
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17: 15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material Was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirrned by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-=TAai!ArN,_S
Sample 12479 FY 1997
METALS SCAN - -
Project: 97-0329 -
THIS TEST SET IS INCOMPLETE
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
ld/Station:JB003SL MD Number: MP72 lnorg Contractor: ANTEC
Media: SOIL
RES UL TS UNITS
7500J MG/KG
0.59UJ MG/KG
0.49UR MG/KG
53J MG/KG
0.69JN MG/KG
3.4JN MG/KG
1600J MG/KG
26J MG/KG
10J MG/KG
21J MG/KG
16000J MG/KG
7.6 MG/KG
4200J MG/KG
370J MG/KG
0.09UJ MG/KG
16J MG/KG
1800J MG/KG
0.32U MG/KG
2.7J MG/KG
370 MG/KG
0.36UJ MG/KG
47J MG/KG
52J MG/KG
14 %
ANALYTE.
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
- -
-Prol!ll!l!ion fl!llf. 1(//'r osW1
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/9718:30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
' ' w:•1·wA~-NAG1:1 __ s ____________ ... __ -Ja11>-'-·--N-l"lll', ... EN-- -
-Pr~on • 1-fl" 09111
Sample 12480 FY 1997 Project: 97-0329 Produced by: Keith Bates
METALS SCAN THIS TEST SET IS INCOMPLETE Requestor: PAT DEROSA
Facilily: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Slation: JB004SL MD Number: MP73
Media: SOIL
SAS Number:TCLP
lnorg Contractor: ANTEC
Project Leader: DEROSA
Beginning: 08/13/97 17:45
Ending:
RESULTS UNITS ANALYTE
13000J MG/KG ALUMINUM
0.51UJ MG/KG ANTIMONY
1.3J MG/KG ARSENIC
83J MG/KG BARIUM
0.99J MG/KG BERYLLIUM
4.1JN MG/KG CADMIUM
1200J MG/KG CALCIUM
27J MG/KG CHROMIUM
13J MG/KG COBALT
29J MG/KG COPPER
20000J MG/KG IRON
72 MG/KG LEAD
3100J MG/KG MAGNESIUM
650J MG/KG MANGANESE
0.11 UJ MG/KG TOTAL MERCURY
19J MG/KG NICKEL
2100J MG/KG POTASSIUM
0.27U MG/KG SELENIUM
2.6J MG/KG SILVER
97 MG/KG SODIUM
0.31UJ MG/KG THALLIUM
53J MG/KG VANADIUM
100J MG/KG ZINC
7 % % MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value glven. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
. ., _,,,,.._.,.::r:NAlafi ---.. --Pro-on !11111-, 09:-
Sample 12481 FY 1997 Project: 97-0329 Produced by: Keith Bates
METALS SCAN THIS TEST SET IS INCOMPLETE
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB005SL MD Number: MP74
Media: SOIL
SAS Number:TCLP
lnorg Contractor: ANTEC
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:00
Ending:
RESULTS UNITS ANALYTE
14000J MG/KG ALUMINUM
0.52UJ MG/KG ANTIMONY
1.5J MG/KG ARSENIC
76J MG/KG BARIUM
0.64JN MG/KG BERYLLIUM
4.2JN MG/KG CADMIUM
4500J MG/KG CALCIUM
28J MG/KG CHROMIUM
8.8J MG/KG COBALT
27J MG/KG COPPER
20000J MG/KG IRON
18 MG/KG LEAD
3300J MG/KG MAGNESIUM
270J MG/KG MANGANESE
0.11 UJ MG/KG TOTAL MERCURY
14J MG/KG NICKEL
2900J MG/KG POTASSIUM
0.28U MG/KG SELENIUM
2.4J MG/KG SILVER
98 MG/KG SODIUM
0.32UJ MG/KG THALLIUM
52J MG/KG VANADIUM
54J MG/KG ZINC
12 % % MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R..qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C--confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-ET ... ArN~S ---Sample 12482 FY 1997 Project: 97-0329
METALS SCAN THIS TEST SET IS INCOMPLETE
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JB006SL MD Number: MP75
Media: SOIL
RESULTS
15000J
0.78UJ
2.2J
82J
0.95JN
5.3JN
4700J
36J
14J
62J
26000J
2300
3500J
510J
0.15UJ
23J
2300J
0.42U
3.5J
820
0.47UJ
68J
180J
38
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
---Pr-ion f!l!II: 1fl', 09.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:00
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
NlllilllS--Sample 12483 FY 1997
METALS SCAN
Project: 97-0329 -
THIS TEST SET IS INCOMPLETE
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
Id/Station: JB007SL MD Number: MP76 lnorg Contractor: ANTEC
Media: SOIL
RESULTS
17000J
0.61UJ
1.9J
88J
0.83JN
5.2JN
1200J
43J
13J
27J
24000J
1100
3200J
650J
0.13UJ
25J
3100J
0.33U
2.9J
70
0.38UJ
54J
110J
21
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
--Produced by: Keith Bales
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presurnptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-1:::l~A N~S-- -
111111\-1
FY 1997 Project: 97-0329
THIS TEST SET IS INCOMPLETE
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
Id/Station: JB008SL MD Number: MP77 lnorg Contractor: ANTEC
Media: SOIL
RESULTS UNITS
13000J MG/KG
0.64UJ MG/KG
0.53UR MG/KG
130J MG/KG
1JN MG/KG
4.5JN MG/KG
710J MG/KG
27J MG/KG
14J MG/KG
27J MG/KG
21000J MG/KG
70 MG/KG
4100J MG/KG
1000J MG/KG
0.14UJ MG/KG
23J MG/KG
4800J MG/KG
0.34U MG/KG
4.2J MG/KG
76 MG/KG
0.39UJ MG/KG
45J MG/KG
77J MG/KG
28 %
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
-Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:35
Ending:
A-average value. NA-not analyzed. NAl-interferences. J--estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampllng and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constiluents or metabolites of technical chlordane
---ill!!IIA -JR:lN ~,-ENl.ll --,.
-Pr-ion-: 1'#17 09. Sample 12485 FY 1997 Project: 97-0329 Produced by: Keith Bates
METALS SCAN THIS TEST SET IS INCOMPLETE
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB009SL MD Number: MP78
Media: SOIL
SAS Number:TCLP
lnorg Contractor: ANTEC
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 21 :45
Ending:
RESULTS UNITS ANALYTE
7500J MG/KG ALUMINUM
1UJ MG/KG ANTIMONY
1UJ MG/KG ARSENIC
87J MG/KG BARIUM
0.54J MG/KG BERYLLIUM
2.7JN MG/KG CADMIUM
960J MG/KG CALCIUM
16J MG/KG CHROMIUM
9.6J MG/KG COBALT
20J MG/KG COPPER
12000J MG/KG IRON
70 MG/KG LEAD
2600J MG/KG MAGNESIUM
710J MG/KG MANGANESE
0.07UJ MG/KG TOTAL MERCURY
15J MG/KG NICKEL
2800J MG/KG POTASSIUM
0.31U MG/KG SELENIUM
1.7J MG/KG SILVER
58 MG/KG SODIUM
0.35U MG/KG THALLIUM
26J MG/KG VANADIUM
71J MG/KG ZINC
8 % %MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
.I ,
It
I
I
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
MEMORANDUM
Date: 11 /26/97
I Subject: Results of METALS INORGANIC Sample Analysis
98-0053 Johnsons Controls Globe
I
I
I ,,
Winston Salem, NC
From: Terri White ~ ~
To: Jennifer Wendel
WMD
CC: Pat DeRosa
NC
Thru: Jenny Scifres ,.:_ S-~--6>
Chief, INORGANIC Chemistry Section
RECEI\/ED
DEC O 8 1997
SUPERFUN0 ::;1::L;\;ON
Attached are the results of analysis of samples collected as part of the subject project. If you have any
ruestions, please contact me.
I
I
ITTACHMENT
I
I
'-I
I
METALS SAMPLE ANALYSIS
Sample 466 FY 1998 Project: 98-0053
METALS SCAN
Facility: Johnsons Controls Globe
Program: SSF
Id/Station: MDMP65
Media: SOIL
RESULTS UNITS ANALYTE
3.0U MG/KG SILVER
6.8 MG/KG ARSENIC
NA MG/KG BORON
100 MG/KG BARIUM
1.5U MG/KG BERYLLIUM
1.5U MG/KG CADMIUM
16 MG/KG COBALT
48 MG/KG CHROMIUM
24 MG/KG COPPER
3.0U MG/KG MOLYBDENUM
14 MG/KG NICKEL
32 MG/KG LEAD
12U MG/KG ANTIMONY
12U MG/KG SELENIUM
7.5U MG/KG TIN
4.0 MG/KG STRONTIUM
15U MG/KG TELLURIUM
1300 MG/KG TITANIUM
30U MG/KG THALLIUM
78 MG/KG VANADIUM
17 MG/KG YTTRIUM
430 MG/KG ZINC
NA MG/KG ZIRCONIUM
Winston Salem, NC
0.0SU MG/KG TOTAL MERCURY
31000 MG/KG ALUMINUM
720 MG/KG MANGANESE
1100 MG/KG CALCIUM
2700 MG/KG MAGNESIUM
35000 MG/KG IRON
300U MG/KG SODIUM
2800 MG/KG POTASSIUM
22 % % MOISTURE
EPA -REGION IV SESD, ATHENS, GA Production Date: 11/26/97 15:31
Produced by: Terri White
Requester: Jennifer Wendel_
Project Leader:
Beginning: 10/29/97 15:35
Ending:·
REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. . K-actuaf value is known to be less than value given. L-actual value is known to be greater than value given ... U-m11;al was analyzed for but not detected. the number is the minimum quantitation lim;,,,t. R-qc indic,=1les that d.sable. compound may or may not be present. resampling and reanalysis is neces verification. --C-<:onfi.y gc'iJa"en-e is _d, se-dan ... tuent-nslit~ met ... o t cht------
METALS SAMPLE ANALYSIS
Sample 467 FY 1998 Project: 98-0053
METALS SCAN
Facility: Johnsons Controls Globe
Program: SSF
Id/Station: MDMP70
Media: SOIL
RESULTS UNITS ANALYTE
2.0U MG/KG SILVER
2.6 MG/KG ARSENIC
NA MG/KG BORON BB MG/KG BARIUM
1.0U MG/KG BERYLLIUM
1.0U MG/KG CADMIUM
12 MG/KG COBALT
36 MG/KG CHROMIUM
21 MG/KG COPPER
2.0U MG/KG MOLYBDENUM
9.2 MG/KG NICKEL
27 MG/KG LEAD
8.0U MG/KG ANTIMONY
8.0U MG/KG SELENIUM
5.0U MG/KG TIN
5.6 MG/KG STRONTIUM
10U MG/KG TELLURIUM
1100 MG/KG TITANIUM
20U MG/KG THALLIUM
48 MG/KG VANADIUM
10 MG/KG YTTRIUM
33 MG/KG ZINC
NA MG/KG ZIRCONIUM
Winston Salem, NC
0.05U MG/KG TOTAL MERCURY
17000 MG/KG ALUMINUM
320 MG/KG MANGANESE
440 MG/KG CALCIUM
2400 MG/KG MAGNESIUM
20000 MG/KG IRON
200U MG/KG SODIUM
1800 MG/KG POTASSIUM
11 % % MOISTURE
EPA -REGION IV SESD, ATHENS, GA
Produced by: Terri White
Requester: Jennifer Wendel
Project Leader:
Beginning: 10/29/97 15:35
Ending:
Production Date: 11/26/97 15:31
REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. K-actual _value is known to be less than value given. L-actual value is known to be weater than valu~ g~ven .. U-m~I wa~ an~lyzed for but not detected. the number is the minimum quantitation tim~,t. R-qc ind1ca!es that da-sable. compound may or may not be present. resamplrng and reanalysis 1s necess venficat1on. -C-confi'.iiiiitygc,.,enililllfeisr.r,selllilllflane-uent-1stitu-met-of. rchrca. ------_,.
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 11/26/97 15:31
Sample 468 FY 1998 Project: 98-0053
METALS SCAN
Facility: Johnsons Controls Globe
Program: SSF
Winston Salem, NC
Produced by: Terri White.
Requester: Jennifer Wendel
Project Leader:
Beginning: 10/29/97 15:35
Ending: Id/Station: MDMP71
Media: SOIL REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
RESULTS UNITS ANALYTE
2.0U MG/KG SILVER
2.5 MG/KG ARSENIC
NA MG/KG BORON
88 MG/KG BARIUM
1.0U MG/KG BERYLLIUM
1.0U MG/KG CADMIUM
13 MG/KG COBALT
35 MG/KG CHROMIUM
21 MG/KG COPPER
2.0U MG/KG MOLYBDENUM
9.3 MG/KG NICKEL
25 MG/KG LEAD
8.0U MG/KG ANTIMONY
8.0U MG/KG SELENIUM
6.5U MG/KG TIN
5.4 MG/KG STRONTIUM
10U MG/KG TELLURIUM
1200 MG/KG TITANIUM
20U MG/KG THALLIUM
48 MG/KG VANADIUM
11 MG/KG YTTRIUM
33 MG/KG ZINC
NA MG/KG ZIRCONIUM
0.05U MG/KG TOTAL MERCURY
16000 MG/KG ALUMINUM
340 MG/KG MANGANESE
420 MG/KG CALCIUM
2400 MG/KG MAGNESIUM
20000 MG/KG IRON
200U MG/KG SODIUM
1800 MG/KG POTASSIUM
11 % % MOISTURE
A-average value. NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is-to be less than value given. L-actual value is known to be greater than value given.Erial was analyzed for but not detected. the-number is th-e minimum-quantitation Ii.
R-qc indicates th nusable. compound may or may not be present. resampling and reanalysis is ne for verification. ..,
C-cc.-dby .wi-aaa,atue-rted,-lord--slilu-con~orrllllite ical-ne ----
METALS SAMPLE ANALYSIS
Sample 469 FY 1998 Project: 98-0053
METALS SCAN
Facility: Johnsons Controls Globe
Program: SSF
Id/Station: MDMP72
Media: SOIL
RESULTS UNITS ANALYTE
3.0U MG/KG SILVER
2.1 MG/KG ARSENIC
NA MG/KG BORON
90 MG/KG BARIUM
1.5U MG/KG BERYLLIUM
1.5U MG/KG CADMIUM
12 MG/KG COBALT
34 MG/KG CHROMIUM
32 MG/KG COPPER
3.0U MG/KG MOLYBDENUM
16 MG/KG NICKEL
13 MG/KG LEAD
12U MG/KG ANTIMONY
15U MG/KG SELENIUM
7.BU MG/KG TIN
16 MG/KG STRONTIUM
15U MG/KG TELLURIUM
1900 MG/KG TITANIUM
30U MG/KG THALLIUM
78 MG/KG VANADIUM
12 MG/KG YTTRIUM
61 MG/KG ZINC
NA MG/KG ZIRCONIUM
Winston Salem, NC
0.05U MG/KG TOTAL MERCURY
22000 MG/KG ALUMINUM
710 MG/KG MANGANESE
3000 MG/KG CALCIUM
6600 MG/KG MAGNESIUM
31000 MG/KG IRON
600 MG/KG SODIUM
3300 MG/KG POTASSIUM
12 % % MOISTURE
EPA -REGION IV SESD, ATHENS, GA
Produced by: Terri White
Requester: Jennifer Wendel
Project Leader:
Beginning: 10/29/97 15:35
Ending:
Production Date: 11/26/97 15:31
REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is-n to be less than v_alue given. l-actual value is known to be greater than value given. Erial was analyzed for but not detected. the number is the minimum quantitation»i
R-qc indicates tha nusable. compound may or may not be present. resampling and reanalysis is nee for verification. -
C-co~ by, .wh-alue -rted, -lorda-stitu ... cons-or aa.te ical ca.,e -----
_ METALS SAMPLE ANALYSIS
Sample 470 FY 1998 Project: 98--0053
METALS SCAN
Facility: Johnsons Controls Globe
Program: SSF
Id/Station: MDMP73
Media: SOIL
RESULTS UNITS ANALYTE
3.0U MG/KG SILVER
4.3 MG/KG ARSENIC
NA MG/KG BORON
130 MG/KG BARIUM
1.SU MG/KG BERYLLIUM
1.5U MG/KG CADMIUM
15 MG/KG COBALT
41 MG/KG CHROMIUM
44 MG/KG COPPER
4.2 MG/KG MOLYBDENUM
19 MG/KG NICKEL
130 MG/KG LEAD
12U MG/KG ANTIMONY
15U MG/KG SELENIUM
7.5U MG/KG TIN
11 MG/KG STRONTIUM
15U MG/KG TELLURIUM
1600 MG/KG TITANIUM
30U MG/KG THALLIUM
85 MG/KG VANADIUM
23 MG/KG YTTRIUM
140 MG/KG ZINC
NA MG/KG ZIRCONIUM
Winston Salem, NC
0.05U MG/KG TOTAL MERCURY
34000 MG/KG ALUMINUM
1100 MG/KG MANGANESE
2100 MG/KG CALCIUM
4900 MG/KG MAGNESIUM
36000 MG/KG IRON
300U MG/KG SODIUM
3400 MG/KG POTASSIUM
35 % % MOISTURE
EPA -REGION IV SESD, ATHENS, GA
Produced by: Terri White
Requester: Jennifer Wendel
Project Leader:
Beginning: 10/29/97 15:35
Ending:
Production Date: 11/26/97 15:31
REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
A-average value. NA-not analyzed. NAl-interferences. J-estlmated value. N-presumptive evidence of presence of material.
K-actual value is.n to be less than value given. L-actual value is known to be greater than value given. -rial was analyzed for but not detected. the number is the minimum quantitation »im·
R-qc indk:ates Iha nusable. compound may or may not be present. resampling and reanalysis is nee for verification.
C-co-by .wh-alue -rted, -lorda.i15titu._,ons-or "111111• ical ca.-,e -------
METALS SAMPLE ANALYSIS
Sample 471 FY 1998 Project: 98-0053
METALS SCAN
Facility: Johnsons Controls Globe Winston Salem, NC
Program: SSF
Id/Station: MDM P74
Media: SOIL
RESULTS UNITS
4.0U MG/KG
5.2 MG/KG
NA MG/KG
120 MG/KG
2.0U MG/KG
2.0U MG/KG
8.6 MG/KG
38 MG/KG
40 MG/KG
8.2 MG/KG
15 MG/KG
23 MG/KG·
16U MG/KG
16U MG/KG
10U MG/KG
26 MG/KG
20U MG/KG
1400 MG/KG
40U MG/KG
77 MG/KG
8.6 MG/KG
68 MG/KG
NA MG/KG
0.05U MG/KG
37000 MG/KG
390 MG/KG
5800 MG/KG
5100 MG/KG
32000 MG/KG
400U MG/KG
5100 MG/KG
10 %
ANALYTE
SILVER
ARSENIC
BORON~
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
MOLYBDENUM
NICKEL
LEAD
ANTIMONY
SELENIUM
TIN
STRONTIUM
TELLURIUM
TITANIUM
THALLIUM
VANADIUM
YTTRIUM
ZINC
ZIRCONIUM
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
EPA -REGION IV SESD, ATHENS, GA
Produced by: Terri White
Requester: Jennifer Wendel
Project Leader:
Beginning: 10/29/97 15:35
Ending:
Production Date: 11/26/97 15:31
REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-pres_umplive evidence of presence of material.
K-actual _value is.n to be less than value given. L-actual value is known to be greater than value given. -rial was analyzed for but not detected. the n-umber is th-e minimum-quantitation»i · R-qc ind!Cales Iha nusab1e. compound may or may not be present. resampling and reanalysis is nee for verification.
C-c~ by .wh-alue-rted,-lord ... stitu-cons-or ~ite ical ca.ne ----
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 11/26/97 15:31
Sample 472 FY 1998 Project: 98--0053
METALS SCAN
Factlity: Johnsons Controls Globe
Program: SSF
Winston Salem, NC
Produced by: Terri While
Requester: Jennifer Wendel
Project Leader:
Beginning: 10/29/97 15:35
Ending: Id/Station: MDMP75
Media: SOIL REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
RESULTS UNITS ANALYTE
4.0U MG/KG SILVER
9.4 MG/KG ARSENIC
NA MG/KG BORON
130 MG/KG BARIUM
2.0U MG/KG BERYLLIUM
2.0U MG/KG CADMIUM
14 MG/KG COBALT
48 MG/KG CHROMIUM
45 MG/KG COPPER
4.0U MG/KG MOLYBDENUM
21 MG/KG. NICKEL
3300 MG/KG LEAD
16U MG/KG ANTIMONY
25U MG/KG SELENIUM
10U MG/KG TIN
21 MG/KG STRONTIUM
20U MG/KG TELLURIUM
1400 MG/KG TITANIUM
40U MG/KG THALLIUM
110 MG/KG VANADIUM
17 MG/KG YTTRIUM
300 MG/KG ZINC
NA MG/KG ZIRCONIUM
0.07 MG/KG TOTAL MERCURY
45000 MG/KG ALUMINUM
860 MG/KG MANGANESE
9000 MG/KG CALCIUM
4100 MG/KG MAGNESIUM
50000 MG/KG IRON
1200 MG/KG SODIUM
3300 MG/KG POTASSIUM
36 % % MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is~n to be less than value given. L-actual value is known to be greater than value given. Eial was analyzed for but not detected. the number is the minimum quantitation~i ·
R-qc indicates tha nusable. compound may or may not be present. resampling and reanalysis is nee for verification. --C-c°lil!llr by .wh-alue-rted, -lorda-stitu .... cons-or ~tes ical ~e -----
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 11/26/97 15:31
Sample 473 FY 1998 Project: 98-0053
METALS SCAN
Facility: Johnsons Controls Globe
Program SSF
Winston Salem, NC
Produced by: Terri White
Requester: Jennifer Wendel
Project Leader:
Beginning: 10/29/97 15:35
Ending: Id/Station: MDMP76
Media: SOIL REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
RESULTS UNITS ANALYTE
4.0U MG/KG SILVER
7.2 MG/KG ARSENIC
NA MG/KG BORON
150 MG/KG BARIUM
2.0U MG/KG BERYLLIUM
2.0U MG/KG CADMIUM
16 MG/KG COBALT
40 MG/KG CHROMIUM
40 MG/KG COPPER
4.0U MG/KG MOLYBDENUM
20 MG/KG NICKEL
1800 MG/KG LEAD
16U MG/KG ANTIMONY
16U MG/KG SELENIUM
10U MG/KG TIN
15 MG/KG STRONTIUM
20U MG/KG TELLURIUM
2100 MG/KG TITANIUM
40U MG/KG THALLIUM
86 MG/KG VANADIUM
18 MG/KG YTTRIUM
160 MG/KG ZINC
NA MG/KG ZIRCONIUM
0.05U MG/KG TOTAL MERCURY
47000 MG/KG ALUMINUM
1200 MG/KG MANGANESE
2200 MG/KG CALCIUM
5000 MG/KG MAGNESIUM
43000 MG/KG IRON
400U MG/KG SODIUM
5500 MG/KG POTASSIUM
18 % % MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actua. I value is~n lo be less than v.alue given. L-actual value is kno.wn to be greater than value given. Erial was analyzed for but not detected. the number is the minimum quantitation~i ·
R-qc indicates Iha nusab!e. compound may or may not be present. resampling and reanalysis is nee for verification. --
C-co-by .wh-alue -rted, -lorda-strtu,..cons-or rraa.te ical clla,e ----
METALS SAMPLE ANALYSIS
Sample 47 4 FY 1998 Project: 98-0053
METALS SCAN
Facilrty: Johnsons Controls Globe
Program: SSF
Id/Station: MDMP77
Media: SOIL
RESULTS UNITS ANALYTE
3.0U MG/KG SILVER
4.1 MG/KG ARSENIC
NA MG/KG .BORON
180 MG/KG BARIUM
1.5U MG/KG BERYLLIUM
1.5U MG/KG CADMIUM
13 MG/KG COBALT
25 MG/KG CHROMIUM
29 MG/KG COPPER
3.0U MG/KG MOLYBDENUM
14 MG/KG NICKEL
94 MG/KG LEAD
12U MG/KG ANTIMONY
12U MG/KG SELENIUM
15U MG/KG TIN
6.1 MG/KG STRONTIUM
15U MG/KG TELLURIUM
2400 MG/KG TITANIUM
30U MG/KG THALLIUM
57 MG/KG VANADIUM
22 MG/KG YTTRIUM
88 MG/KG ZINC
NA MG/KG ZIRCONIUM
Winston Salem, NC
0.05U MG/KG TOTAL MERCURY
30000 MG/KG ALUMINUM
1500 MG/KG MANGANESE
850 MG/KG CALCIUM
5400 MG/KG MAGNESIUM
32000 MG/KG IRON
300U MG/KG SODIUM
6900 MG/KG POTASSIUM
7 % % MOISTURE
EPA -REGION IV SESD, ATHENS, GA
A-average value. NA-not analyzed. NAl-inlerterences. J-estimated value. N-presumptive evidence or presence of material.
Produced by: Terri White
Requester: Jennifer Wendel
Project Leader:
Beginning: 10/29/97 15:35
Ending:
Production Date: 11/26197 15:31
REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
R-qc inCicates th.unusable. compound may or may not be present. resampling and reanalysis is ne for verification.
K-actual value is known to be less than vatue given. L-aclual value is known to be greater than value given. terial was analyzed for but not detected. then-umber is th-e minimum-quantitation»i · C-c-by ra, .wh-alueilllfrted,.lord ... stitu-con'11111W or "llill'te ical ca.n• ----
METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA Production Date: 11/26/97 15:31
Sample 475 FY 1998 Project: 98-0053
METALS SCAN
Facility: Johnsons Controls Globe
Program: SSF
Winston Salem, NC
Produced by: Terri White
Requester: Jennifer Wendel
Project Leader:
Beginning: 10/29/97 15:35
Ending: Id/Station: MDMP78
Media: SOIL REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
RESULTS UNITS ANALYTE
3.0U MG/KG SILVER
1.8 MG/KG ARSENIC
NA MG/KG BORON
130 MG/KG BARIUM
1.5U MG/KG BERYLLIUM
1.5U MG/KG CADMIUM
11 MG/KG COBALT
22 MG/KG CHROMIUM
23 MG/KG COPPER
3.0U MG/KG MOLYBDENUM
14 MG/KG NICKEL
80 MG/KG LEAD
12U MG/KG ANTIMONY
12U MG/KG SELENIUM
7.5U MG/KG TIN
4.7 MG/KG STRONTIUM
15U MG/KG TELLURIUM
1600 MG/KG TITANIUM
30U MG/KG THALLIUM
49 MG/KG VANADIUM
19 MG/KG YTTRIUM
77 MG/KG ZINC
NA MG/KG ZIRCONIUM
0.05U MG/KG TOTAL MERCURY
23000 MG/KG ALUMINUM
1100 MG/KG MANGANESE
880 MG/KG CALCIUM
3900 MG/KG MAGNESIUM
26000 MG/KG IRON
300U MG/KG SODIUM
4500 MG/KG POTASSIUM
9 % % MOISTURE
A-average value. NA-not analyzed. NAl-interierences. J-estimated value. N-presumptive evidence of presence or material.
K-actual value is-to be less than value given. L-actual value is known to be greater than value given .. llE"al was analyzed for but not detected. the -number is th-e minimum-quantitation lim.A
R-qc inC;cates tha nusable. compound may; may not ~e pres~nt.,sampling and reanalysis is nee for veri~. -..,
C-c-by .wttllll-'alue-rted, lord stitu .con~ or ~1tes ical ~ne ---
,I
'9
I
I
I
MEMORANDUM
Date: 11/14/97
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I Subject: Results of METALS INORGANIC Sample Analysis
RECF!\IED
NOV 18 1997
SUPERFUND SECTl0~1
I
I
I ,
97-0328 JOHNSON CONTROLS GLOBE
From: Keith Bates
WINSTON-SALEM, NC
;::_ .d IS Jc:::::::'
To: PAT DEROSA
Thru: QA Office
Attached are the results of analysis of samples collected as part of the subject project. If you have any
tuestions, please contact me.
I
I
lnACHMENT
I
I
It
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
INORGANIC DATA QUALIFIERS REPORT
Case Number:_.=6~3,,_,,3 ________________ _
Project Number:_a9~7~-~0~3=2~Bc_ _____________ _
Site: Johnson·Controls Globe, Winston-Salem, NC
Element Flag
A. Waters
Cr, Cu u
Al, Ca, Fe, Mg, u
K, Zn
Na ·J
Na J
V u
Pb J
Co J
Pb J
Mn J
Ni J
V J
B. Soils
Cr, Cu u
Al,. Ca, Fe, Mg, u
K, Zn
Pb JN
Se JN
Samples Affected
All positives > IDL, but
< CRDL
All positives > IDL, but
< CRDL
12453, 12457, 12458, 12459,
12460, 12461
12412, 12415, 12416, 12419,
12420, 12422, 12423, 12425,
12427, 12 42 9, 12431, 12434,
12436, 12438, 12441, 12442,
12447, 12 4 4 9, 12451
12412, 12416, 12429, 12438,
12442
12416
12434, 12448
12419, 12420
12457
12420, 12423, 12425, 12438,
12441, 12447, 12448, 12451
12419, 12420, 12423, 12425,
12427, 12441, 12447, 12451
12458
All positives> IDL, but
< CRDL
All positives> IDL, but
< CRDL
12413, 12417, 12435
12413, 12435
Reason
Baseline instability
Positives in blanks
Serial dilution percent difference=
14.6%
serial dilution percent difference=
10.1%
% RSD > 20% for ICP multiple exposures
and results> IDL, but< CRDL
% RSD >
exposures
20% for ICP multiple
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
Only · analysis of 2X CRDL standard
required by contract sow for ICP
analysis
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Baseline instability
Positives in blanks
Suspected positive interference as
noted in the contractor res
Suspected positive interference as
noted in the contractor res
I
It
I
I
I
I
I
I
I ,
I
I
I
I
I
I
'-I
I
INORGANIC DATA QUALIFIERS REPORT (continued)
Case Number:_.2~5~6~3~3,,._ _______________ _
Project Number:_,9~7~-~0~3=2~8 ______________ _
Site: Johnson Controls Globe, Winston-Salem, NC
Element Flag
Na J
Cr J
Zn J
Sb u.
As u
Ag u
Tl u
As J
Se J
Tl J
Sb J
As J
Be J
Samples Affected
12413, 12414, 12417, 12418,
12421, 12424, 12426, 12428,
12430, 12432, 12433, 12435,
12437, 12439, 12440, 12443,
12444, 12445, 12446, 12448,
12450, 12452, 12454, 12455,
12456
12448, 12450, 12452, 12454,
12455, 12456
12448, 12450, 12452, 12454,
12455, 12456
12456
12439
12418
12417, 12418, 12421, 12440
12414, 12433, 12444, 12456
12414, 12440, 12444
12456
12413, 12414, 12417, 12418,
12424, 12433, 12435, ·12439,
12444, 12445, 12446,
12448
12421, 12424, 12426, 12428,
12430, 12432, 12433, 12435,
12437, 12439, 12 4 4 0, 12443,
12 4 4 4, 12445, 12 4 4 6, 12448,
12450, 12452, 12454, 12455,
12456
Reason
Blirid spike recovery> action limit
Serial dilution percent difference=
12.6%
Serial dilution percent difference
20.5%
% RSD > 20% for ICP multiple exposures
and results> IDL, but< CRDL
% RSD > 20% for ICP multiple exposures
and results> IDL, but< CRDL
% RSD > 20% for ICP multiple exposures
and results> IDL, but< CRDL
% RSD > 20% for ICP multiple exposures
and results> IDL, but< CRDL
% RSD > 20%
exposures
% RSD >
exposures
% RSD >
exposures
20%
20%
for ICP multiple
for ICP multiple
for ICP multiple
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
_I
I
I
I
I
I
I ,
I
I
I
I
I
I
I
INORGANIC DATA QUALIFIERS REPORT (continued)
Case Number:_.~5~6~3~3.,_ _______________ _
Project Nwnber:--"9~7_-~0~3~2"-"8 ______________ _
Site: Johnson controls Globe, Winston-Salem, NC
Element
Co
Ni
Se
Ag
Tl
Flag
J
J
J
J
J
Samples Affected
12414, 12421, 12424, 12428,
12430, 12432, 12433, 12435,
12437, 12439, 12440, 12443,
12444, 12450, 12452, 12454,
12455
12424, 12426, 12428, 12432,
12435, 12439, 12444, 12446,
12450, 12452, 12454, 12455
12414, 12440, 12444
12417, 12426, 12445
12413, 12414, 12424, 12433,
12445
Reason
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
Only analysis
required by
analysis
of 2X CRDL standard
contract sow for ICP
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
METALS SAMPLE ANALYSIS
Sample 12459 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC001 FB MD Number: MP82
Media: WATER
RESULTS. UNITS
2U UG/L
7U UG/L
1U UG/L
1U UG/L
1U UG/L
2U UG/L
1U UG/L
1U UG/L
1U UG/L
2U UG/L
5U UG/L
5U UG/L
6U UG/L
1U UG/L
2U UG/L
0.20U UG/L
40U UG/L
1U UG/L
30U UG/L
23U UG/L
22U UG/L
40J UG/L
30U UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:45
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number 1s the minimum qu;,,n n limit
R-qc indicates t~-unusable. compound may or may not be present. resampling and reanalysis -·s~ary for verification. .
C-\o.._d by ~,_w_ valuiiiporte'-i chto-cons-2.c.entsliit~techrlliflordilill ------
METALS SAMPLE ANALYSIS
Sample 12460 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC001 PB MD Number: MP83
Media: WATER
RESULTS
2U
7U
1U
1U
1U
2U
1U
1U
1U
2U
SU
SU
6U
1U
2U
0.20U
40U
1U
12U
23U
22U
27UJ
19U
UNITS
UG/L
UG/L ·
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 14:00
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number 1s the minimum qu;Jjnt n hm1t
R-qc indicates t-a unusable. compound may or may not be present. resarnpling and reanalysis i"'sary for verification.
C-confirmed by gc .when no value is reported, see chlordane cons~s 2.constituents or meta tech~lord~ -----~-______ ,_ ---
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12461 FY 1997 Project: 97 -0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC002PB MD Number: MP84
Media: WATER
RESULTS
2U
7U
1U
1U
1U
2U
1U
1U
1U
2U
5U
5U
BU
1U
2U
0.20U
30U
1U
12U
23U
22U
27UJ
19U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 21 :20
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detect-ed. the num-ber is the -minimum qu;Jlntl · n 1-imit.
R-qc indicates t~!-unusable. compound may or may not be present. resampling and reanalysis i-s-~ary for verification.
C-co .. d by -.w __ valu-porte .. chto ... constituenfs 2.c .. ents or m;ta~tech-lordliill -
METALS SAMPLE ANALYSIS
Sample 12455 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC011 SL MD Number: MP66
Media: SOIL D Number: MP66
RESULTS UNITS ANALYTE
0.54U MG/KG SILVER
2.8 MG/KG ARSENIC
91 MG/KG BARIUM
0.77J MG/KG BERYLLIUM
0.27U MG/KG CADMIUM
9.6J MG/KG COBALT
22J MG/KG CHROMIUM
15 MG/KG COPPER
9.6J MG/KG NICKEL
32 MG/KG LEAD
1.3U MG/KG ANTIMONY
1.3U MG/KG SELENIUM
1.6U MG/KG THALLIUM
48 MG/KG VANADIUM
44J MG/KG ZINC
0.13U MG/KG TOTAL MERCURY
22000 MG/KG ALUMINUM
480 MG/KG MANGANESE
870 MG/KG CALCIUM
1700 MG/KG MAGNESIUM
24000 MG/KG IRON
140J MG/KG SODIUM
1500 MG/KG POTASSIUM
25 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 16:25
Ending:
Production Date: 11/14/97 07:34
R-qc indicates !~~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number 1s the mmunum qu;Jlnt n l1m1t
C-co.d by .,.w_ valu-ortellii chlo1illf'ns-2.c.ents-a tech'illtlord-------
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12456 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC012SL MD Number: MP67
Media: SOIL D Number: MP67
RESULTS UNITS ANALYTE
0.56U MG/KG SILVER
3.3J MG/KG ARSENIC
120 MG/KG BARIUM
1.1J MG/KG BERYLLIUM
0.28U MG/KG CADMIUM
18 MG/KG COBALT
35J MG/KG CHROMIUM
31 MG/KG COPPER
19 MG/KG NICKEL
51 MG/KG LEAD
2U MG/KG ANTIMONY
1.4U MG/KG SELENIUM
3J MG/KG THALLIUM
79 MG/KG VANADIUM
200J MG/KG ZINC
0.14U MG/KG TOTAL MERCURY
32000 MG/KG ALUMINUM
1100 MG/KG MANGANESE
1400 MG/KG CALCIUM
3300 MG/KG MAGNESIUM
40000 MG/KG IRON
190J MG/KG SODIUM
3500 MG/KG POTASSIUM
31 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:56
Ending:
Production Date: 11/14/97 07:34
K-actuat value is known to be less than value given. L-actual value is known to be weater than valu~ ~iven. U-material w~~ a~alyzed for but not detected. the number 1s the minimum quJlnt on hrrnt
R-qc indicates t~-unusable. compound may or may not be present. resamphng and reanalysis 1-s-~ary for venf1cat10n.
C-c-d by •. w ... valu .. porte ... chlo ... consas 2.c1111111ents-ta,Wtech-lord. -----..
METALS SAMPLE ANALYSIS
Sample 12444 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC013SL MD Number: MP54
Media: SOIL D Number: MP54
RESULTS UNITS ANALYTE
0.49U MG/KG SILVER
2J MG/KG ARSENIC
68 MG/KG BARIUM
0.72J MG/KG BERYLLIUM
2.2 MG/KG CADMIUM
7.7J MG/KG COBALT
31 MG/KG CHROMIUM
15 MG/KG COPPER
8.7J MG/KG NICKEL
120 MG/KG LEAD
2J MG/KG ANTIMONY
1.5J MG/KG SELENIUM
1.5U MG/KG THALLIUM
47 MG/KG VANADIUM
250 MG/KG ZINC
0.13U MG/KG TOTAL MERCURY
20000 MG/KG ALUMINUM
260 MG/KG MANGANESE
670 MG/KG CALCIUM
2300 MG/KG MAGNESIUM
23000 MG/KG IRON
130J MG/KG SODIUM
2400 MG/KG POTASSIUM
21 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estirnated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :50
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detect-ed. the num-ber is the-minimum q":Jjan · ion 1-imit.
R-qc indicates t~-unusable. compound may or m_ay not be present. resampling and reanalysis ~s-~ary for verification.
C--ed by ,.1.w .. o valuiiiportedj see chlo. cons-s 2.consfif uents·t~ tech-hlord---
METALS SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA
Sample 12445 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC014SL MD Number: MP55
Media: SOIL D Number: MP55
RESULTS UNITS ANALYTE
0.53J MG/KG SILVER
1.7U MG/KG ARSENIC
84 MG/KG BARIUM
0.91J MG/KG BERYLLIUM
0.25U MG/KG CADMIUM
14 MG/KG COBALT
38 MG/KG CHROMIUM
25 MG/KG COPPER
16 MG/KG NICKEL
190 MG/KG LEAD
2.4J MG/KG ANTIMONY
1.2U MG/KG SELENIUM
1.5J MG/KG THALLIUM
51 MG/KG VANADIUM
72 MG/KG ZINC
0.12U MG/KG TOTAL MERCURY
20000 MG/KG ALUMINUM
560 MG/KG MANGANESE
720 MG/KG CALCIUM
3000 MG/KG MAGNESIUM
25000 MG/KG IRON
180J MG/KG SODIUM
2800 MG/KG POTASSIUM
18 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COM PU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 15:45
Ending:
Production Date: 11/14/97 07:34
K-actuat value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum q~an ·on hmit
R-qc indicates t~~-unusable. compound may or may not be present. resampling and reanalysis i•s-~ary for verification.
C-c-dby •. w ... valuiiiporte-chlo.consas 2.c11111uentsormeta~tech-hlord. ~ ----
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12442 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC001 SW MD Number: MP52
Media: SURFACEWA D Number: MP52
RES UL TS UNITS ANALYTE
2U UG/L SILVER
7U UG/L ARSENIC
41 UG/L BARIUM
1U UG/L BERYLLIUM
1U UG/L CADMIUM
2U UG/L COBALT
1U UG/L CHROMIUM
SU UG/L COPPER
1U UG/L NICKEL
2U UG/L LEAD
SU UG/L ANTIMONY
SU UG/L SELENIUM
6U UG/L THALLIUM
2U UG/L VANADIUM
7U UG/L ZINC
0.20U UG/L TOTAL MERCURY
160U UG/L ALUMINUM
33 UG/L MANGANESE
6900 UG/L CALCIUM
2500 UG/L MAGNESIUM
340 UG/L IRON
5400J UG/L SODIUM
1400 UG/L POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :00
Ending:
Production Date: 11/14/97 07:34
R--qc indicates t~~-unusable. compound may or may not be present. resamphng and reanalysis I ssary for verification.
K-actual_value is known to be less than value given. L-actual value is known to be weater than valu~ ~-·ve. LI-material w~s a~alyzed for but not detected. the number 1s the minimum q":Jlan n l1m1t
C-c-ed by .... w111110 valu~portelflii chlo-cons-s 2 .• uents-ta tech-hlordlil ------
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12443 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC001 SD MD Number: MP53
Media: SEDIM D Number: MP53
RESULTS UNITS ANALYTE
0.70U MG/KG SILVER
2.5U MG/KG ARSENIC
120 MG/KG BARIUM
1.3J MG/KG BERYLLIUM
0.35U MG/KG CADMIUM
12J MG/KG COBALT
31 MG/KG CHROMIUM
25 MG/KG COPPER
15 MG/KG NICKEL
24 MG/KG LEAD
1.8U MG/KG ANTIMONY
1.8U MG/KG SELENIUM
2.1U MG/KG THALLIUM
48 MG/KG VANADIUM
71 MG/KG ZINC
0.17U MG/KG TOTAL MERCURY
20000 MG/KG ALUMINUM
490 MG/KG MANGANESE
1200 MG/KG CALCIUM
4400 MG/KG MAGNESIUM
22000 MG/KG IRON
190J MG/KG SODIUM
4400 MG/KG POTASSIUM
44 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :30
Ending:
Production Date: 11/14/97 07:34
R-qc indicates !~~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv. U-material was analyzed for but not detected. the number 1s the minimum q~an n hmit
C-c-d by., w-valwport'ailii chlo-consw 2 .• ent .. ta techilliiilW'lord.. ------
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 1244 7 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC002SW MD Number: MP57
Media: SURFACEWA
RESULTS
2U
?U
17
1U
1U
2U
SU
4U
3J
2U
SU
SU
6U
4J
BU
0.20U
?BOU
500
6400
2400
1800
4100J
1800
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MP57
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:45
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv. U-material was analyzed for but not detected. the number 1s the m1mmum q;,,an · n limit
R-qc indicates~~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-c-edby,.,,.w.vahilifportiiifrchl-con-s 2 .• uent'Mta tech-hlordilll ----.. -
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12446 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC002SD MD Number: MP56
Media: SEDIM D Number: MP56
RESULTS UNITS ANALYTE
3.8 MG/KG SILVER
2U MG/KG ARSENIC
160 MG/KG BARIUM
0.76J MG/KG BERYLLIUM
0.29U MG/KG CADMIUM
21 MG/KG COBALT
21 MG/KG CHROMIUM
15 MG/KG COPPER
9.5J MG/KG NICKEL
25 MG/KG LEAD
1.9J MG/KG ANTIMONY
3.1 MG/KG SELENIUM
1.8U MG/KG THALLIUM
33 MG/KG VANADIUM
91 MG/KG ZINC
0.13U MG/KG TOTAL MERCURY
14000 MG/KG ALUMINUM
5600 MG/KG MANGANESE
920 MG/KG CALCIUM
2000 MG/KG MAGNESIUM
21000 MG/KG IRON
130J MG/KG SODIUM
1800 MG/KG POTASSIUM
32 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 12:30
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number 1s the mrnimum qu;,,n · n limit
R-qc indicates I~~-unusable. compound may or may not be present. resampling and reanalysis i-ss_ary for verification. C-co-d by -.w1111111 valu-porteilii chlo-ons-2.c.ents .a,..techwlord-------
METALS SAMPLE ANALYSIS
Sample 12448 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC003SD MD Number: MP58
Media: SEDIM D Number: MP58
RESULTS UNITS ANALYTE
0.51U MG/KG SILVER
2J MG/KG ARSENIC
69 MG/KG BARIUM
0.62J MG/KG BERYLLIUM
0.26U MG/KG CADMIUM
5.9J MG/KG COBALT
16J MG/KG CHROMIUM
9.2 MG/KG COPPER
6.7J MG/KG NICKEL
52 MG/KG LEAD
1.3U MG/KG ANTIMONY
1.3U MG/KG SELENIUM
1.5U MG/KG THALLIUM
24 MG/KG VANADIUM
49J MG/KG ZINC
0.13U MG/KG TOTAL MERCURY
7000 MG/KG ALUMINUM
460 MG/KG MANGANESE
460 MG/KG CALCIUM
2000 MG/KG MAGNESIUM
13000 MG/KG IRON
110J MG/KG SODIUM
2000 MG/KG POTASSIUM
25 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :15
Ending:
Production Date: 11/14/97 07:34
R-qc indicates~~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value gl&iiv. LI-material was analyzed for but not detected. the number 1s the minimum q":Jjan n 11m1t
C-c-ed by...,,,, .w. val-portllllii chlo-con-s 2 .• ent'Mta tech-hlordilll ----IBI -
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12449 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC004SW MD Number: MP59
Media: SURFACEWA D Number: MP59
RESULTS
2U
7U
36
1U
1U
2U
1U
5U
1U
22
5U
5U
6U
1U
20U
0.20U
200U
270
5200
2500
630
6700J
1700
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 10:05
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actuat value is known to be less than value given. L-actual value is known to be greater than value g~iv Li-material was analyzed for but not detected. the number is the minimum q;,,an ·· · n limit.
R-qc indicates thaA unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-c-dby..,,.w.valWport'llllii'chl<tllllconsliilW 2 . .,ent,..ta tech~lord-------
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12450 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC004SD MD Number: MP60
Media: SEDIM D Number: MP60
RESULTS UNITS ANALYTE
0.61U MG/KG SILVER
2.1U MG/KG ARSENIC
88 MG/KG BARIUM
0.91J MG/KG BERYLLIUM
0.30U MG/KG CADMIUM
6.4J MG/KG COBALT
29J MG/KG CHROMIUM
15 MG/KG COPPER
10J MG/KG NICKEL
340 MG/KG LEAD
1.5U MG/KG ANTIMONY
1.5U MG/KG SELENIUM,
1.8U MG/KG THALLIUM
36 MG/KG VANADIUM
56J MG/KG ZINC
0.14U MG/KG TOTAL MERCURY
13000 MG/KG ALUMINUM
140 MG/KG-MANGANESE
920 MG/KG CALCIUM
2900 MG/KG MAGNESIUM
13000 MG/KG IRON
160J MG/KG SODIUM
2600 MG/KG POTASSIUM
35 % % MOISTURE
I norg Contractor: CH EM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13197 10:30
Ending:
Production Date: 11/14/97 07:34
R-qc indicates !~~-unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g-ive LI-material was analyzed for but not detected. the number 1s the minimum qu;Jlnt n l1m1t
C-c-dbyi9'w-valu-port ... chlo-onsw 2 .• ents-ta tech,.,lord-----. --
METALS SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA
Sample 12451 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC005SW MD Number: MP61
Media: SURFACEWA D Number: MP61
RESULTS
2U
7U
33
1U
1U
2U
1U
7U
1J
2U
5U
5U
6U
6J
BU
0.20U
590U
24
6400
2100
850
7200J
1300
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 12:05
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number 1s the m1n1mum q;Jlant on l1m1t
R-qc indicates t~a-unusable. compound may or may not be present. resampling and reanalysis i-s~ary for verification.
C-c-ed by.,,.w. valuilii'porteiilaiii chlo-consiil!if 2 .• entsMta~tech-hlord.. ------
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12452 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC005SD MD Number: MP62
Media: SEDIM
RES UL TS UNITS
0.56U
2U
38
0.60J
0.28U
2.9J
17J
8
6.1J
7.4
1.4U
1.4U
1.7U
15
18J
0.14U
5100
51
880
1100
4900
120J
650
30
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MP62
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/9712:35
Ending:
Production Date: 11/14/97 07:34
R-qc indicates !~:-unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number 1s the mm1mum qu~n · n hm1t
C-confirmed by .,.wh-valu-orteiiilichlor-onst-2.c.ents -• ech'illlllord,.. ------
METALS SAMPLE ANALYSIS
Sample 12422 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC006SW MD Number: MH94
Media: SURFACEWA
RESULTS
2U
7U
32
1U
1U
2U
1U
4U
1U
5
SU
SU
6U
1U
7U
0.20U
210U
360
5700
2300
2600
5500J
1400
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MH94
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumplive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 12:25
Ending:
Production Date: 11/14/97 07:34
R-qc indicates t~~-unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number 1s the minimum qu";Jlnt n l1m1t C-c-d by,. w-val-port .... chlo-consw 2.'ilii'ents-ta tech'lllii'lord-------
METALS SAMPLE ANALYSIS
Sample 12423 FY 1997
METALS SCAN
_ EPA· REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC106SW MD Number: MH95
Media: SURFACEWA
RESULTS UNITS
2U UG/L
7U UG/L
32 UG/L
1U UG/L
1U UG/L
2U UG/L
4U UG/L
4U UG/L
3J UG/L
5 UG/L
SU UG/L
SU UG/L
6U UG/L
1J UG/L
20U UG/L
0.20U UG/L
200U UG/L
350 UG/L
5600 UG/L
2300 UG/L
2500 UG/L
5400J UG/L
1300 UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MH95
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 12:30
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number 1s the mm1mum qu;Jjnt1 n 11m1t
R-qc indicates t~~-unusable. compound may or may not be present. resampling and reanalysis i~~ary for verification.
C-';°-dby.,.whennovalu-porteiiliiiichlo-cons-2 .• ents-ta~techwlord.. -----
--~ -
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample · 12424 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC006SD MD Number: MH96
Media: SEDIM
RESULTS
1.6U
5.6U
240
2.1J
0.80U
26J
60
49
30J
300
SJ
4U
6.4J
93
130
0.38U
50000
1400
1800
4200
73000
250J
3400
76
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MH96
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 13:00
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value giv-U-material was analyzed for but not detected. the number 1s the minimum qu;J/lntt l1m1t
R-qc indicates t~~-unusable. compound may or may not be present. resampling and reanalysis is sary for verification.
C-co-dby~.w-valu-orteiliiichlo-cons-2 .• ents-ab tech'illtlord-------
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12434 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC007SW MD Number: MK09
Media: SURFACEWA D Number: MK09
RESULTS
2U
7U
74
1U
1U
2J
1U
3U
1U
2U
SU
SU
6U
1U
20U
0.20U
120U
1700
8500
2600
16000
4000J
1400
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:26
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actua1 value is known to be less than value given. L-actual value is known to be greater than value g~iv Li-material was analyzed for but not detected. the number 1s the minimum q;/lan n J1m1t
R-qc indicates t~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-c-edby~·"iiirval'ililfportllllchl-con-s 2 . .,ent'lllla'ta tech-hlor'1all ------
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12436 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Stalion:JC107SW MD Number: MK11
Media: SURFACEWA D Number: MK11
RESULTS UNITS ANALYTE
2U UG/L SILVER
7U UG/L ARSENIC
72 UG/L BARIUM
1U UG/L BERYLLIUM
1U UG/L CADMIUM
2U UG/L COBALT
1U UG/L CHROMIUM
1U UG/L COPPER
1U UG/L NICKEL
2U UG/L LEAD
5U UG/L ANTIMONY
5U UG/L SELENIUM
6U UG/L THALLIUM
1U UG/L VANADIUM
9U UG/L ZINC
0.20U UG/L TOTAL MERCURY
90U UG/L ALUMINUM
1600 UG/L MANGANESE
8300 UG/L CALCIUM
2500 UG/L MAGNESIUM
15000 UG/L IRON
3900J UG/L SODIUM
1300 UG/L POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:26
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g.ive. LI-material was analyzed for but not detected. the number 1s the mm1mum q:,,ant n limit
R-qc indicates t~:a unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-c .. edby...,.w.ova1u-port~chlo-cons-2 .• ent5Mta techifiiltlordiilll ------
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12435 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC007SD MD Number: MK10
Media: SEDIM D Number: MK10
RES UL TS UNITS ANALYTE
0.93U MG/KG SILVER
5.9 MG/KG ARSENIC
170 MG/KG BARIUM
1.7J MG/KG BERYLLIUM
0.46U MG/KG CADMIUM
14J MG/KG COBALT
40 MG/KG CHROMIUM
31 MG/KG COPPER
18J MG/KG NICKEL
34JN MG/KG LEAD
5.1J MG/KG ANTIMONY
2.7JN MG/KG . SELENIUM
2.8U MG/KG THALLIUM
73 MG/KG VANADIUM
97 MG/KG ZINC
1.1 MG/KG TOTAL MERCURY
43000 MG/KG ALUMINUM
550 MG/KG MANGANESE
1200 MG/KG CALCIUM
2800 MG/KG MAGNESIUM
71000 MG/KG IRON
200J MG/KG SODIUM
2200 MG/KG POTASSIUM
69 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:55
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value givE!n. L-actual value is known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum q;Jlan · limit.
R-qc indicates Iha.unusable. compound may or may not be present. resampling and reanalysis i sary for verification. C-cad by..,.w. val,.port ... chl~cons_. 2.'lilllii'ent,..tab tech_,lord-------
METALS SAMPLE ANALYSIS
Sample 12438 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC008SW MD Number: MK13
Media: SURFACEWA
RESULTS
2U
7U
24
1U
1U
2U
4U
3U
3J
2U
5U
5U
6U
2U
6U
0.20U
190U
350
6000
2400
1300
4500J
1400
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MK13
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 19:25
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estlmated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value ls known to be greater than value g~iv U-material was analyzed for but not detected. the number is the minimum q;Jlan · limit.
R-qc indicates !~:-unusable. compound may or may not be present. resampling and reanalysis i sary for verification. ·
C--dby__,w.val-port-chl-consw 2 . .,ent ... tab tech_,lord-------
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12437 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC008SD MD Number: MK12
Media: SEDIM D Number: MK12
RESULTS UNITS ANALYTE
0.67U MG/KG SILVER
2.4U MG/KG ARSENIC
120 MG/KG BARIUM
1.3J MG/KG BERYLLIUM
0.34U MG/KG CADMIUM
13J MG/KG COBALT
34 MG/KG CHROMIUM
20 MG/KG COPPER
14 MG/KG NICKEL
15 MG/KG LEAD
1.7U MG/KG ANTIMONY
1.7U MG/KG SELENIUM
2U MG/KG THALLIUM
52 MG/KG VANADIUM
69 MG/KG ZINC
0.16U MG/KG TOTAL MERCURY
26000 MG/KG ALUMINUM
570 MG/KG MANGANESE
1100 MG/KG CALCIUM
3300 MG/KG MAGNESIUM
26000 MG/KG IRON
180J MG/KG SODIUM
2800 MG/KG POTASSIUM
42 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
Production Date: 11/14/97 07:34
R-qc indicates t~~-unusable. compound may or may not be present. re sampling and reanalysis i~~ary for verification. .
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number 1s the minimum q;Jlant1 n limit
C-c-dby..,..wliiivaluiiiported seechlo-cons-2.c.entsiiita~techwlord.. ------
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12439 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC108SD MD Number: MK14
Media: SEDIM
RESULTS
0.65U
3U
110
1.2J
0.32U
11J
30
19
12J
14
2J
1.6U
1.9U
47
62
0.16U
21000
520
910
2900
23000
170J
2400
39
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MK14
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual.value is known to be less than value given. L-actual value is known to be weater than valu~ ~~·v Li-material w~s a~alyzed for but not detected. the number 1s the minimum q;J/la n limit
R-qc indicates_ t~-unusable. compound may or may not be present. resampllng and reanalysis I ssary for verification. C-edbi9" .• ovalllifpo1ilifchl-con-ts 2-uent .. ta ftec~hlor-------
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12441 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC009SW MD Number: MP51
Media: SURFACEWA
RESULTS
2U
7U
27
1U
1U
2U
15
20U
BJ
2U
SU
SU
6U
1J
SU
0.34
230
370
6400
2600
1800
5300J
1500
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MP51
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:45
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~ive U-material was analyzed for but not detected. the number 1s the minimum qu;Jln n limit
R-qc indicates !~~unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-c-dby~.w-valu-porte .. chlo-consw 2 .• ents-ta tech-lord-------
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12440 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC009SD MD Number: MP50
Media: SEDIM
RESULTS
0.80U
2.8U
160
1.9J
0.40U
18J
49
28
21
22
4U
2.3J
4U
74
100
0.21U
38000
930
1300
4000
40000
250J
3400
53
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MP50
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAf-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:30
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-materiat was analyzed for but not detected. the number 1s the minimum q;J;an on hm1t
R-qc indlcates .. t~a-unusable. compound may or may not be present. resampling and reanalysis i-ssary for verification.
C-confirmed biilll', .• o val-eportiiliie chi-con-ts 2 .• tuent-eta'Wjf tec-hlor'liil ------
METALS SAMPLE ANALYSIS EPA -R.[GIQ.:, IV SESD, ATHENS, GA
Sample 12453 FY 1997 Project: 97 -0328
METALS SCA_N .
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC010SW MD Number: MP63
Media: SURFACEWA D Number: MP63
RESULTS
2U
7U
30
1U
1U
2U
1U
1U
1U
2U
5U
5U . 6U
1U
2U
0.20U
60U
34
4900
2300
210U
2500J
1000
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM·
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estlmated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 09:40
Ending:
Production Date: 11/14/97 07:34
R-qc indicates th unusable. compound may or may not be present. resarnpling and reanalysis ssary for verification.
K-actual valuea·s kn wn to be less than value given. L-actual value is known to be greater than va!ue ~i. LI-material was analyzed for but not detected. the number 1s ttie m1nimum;,,uan 10n l1m1t
C--edb· . .,ovc-epo~-ech-•co,.-,ts Wituer-et fte'tlillichlo-------
METALS SAMPLE ANALYSIS
Sample 12454 FY 1997
METALS SCAN -----
EPA -REGION IV SESD, ATHENS, GA
Project 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC010SD MD Number: MP64
Media: SEDIM
RESULTS
0.52U
1.8U
80
1J
0.26U
8.1J
25J
9.7
7.8J
6.8
1.3U
1.3U
1.6U
31
25J
0.14U
8500
240
550
1700
13000
130J
1200
26
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MP64
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 09:25
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual valu~is wn to be fess than value given. L-actual value is known to be greater than value-.· en. U-material was analyzed for but not detected.
R-qc indicates t a unusable. compound may or may not be present. resampling and reanalysi cessary for verification.
ca.med lllill no 1illi rep...,ee "illilne "'llll'nts -titu'liliilme oft-al chi--1!11!1
Production Date: 11/14/97 07:34
-
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12429 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC011 SW
Media: SURFACEWA
RESULTS
2U
7U
29
1U
1U
2U
1U
4U
1U
2U
5U
5U
6U
2U
5U
0.20U
180U
23
5900
3000
560
3800J
1000
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: MJ01
D Number: MJ01
TOTAL MERCURY
ALUMINUM
MANGANESE
CAlCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:25
Ending:
A-average value. NA-not analyzed. NA1-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual valu~is wn to be less than value given. L-actual value is known to be greater than valu~: n. U-material was analyzed for but not detected.
R-qc indicates ta unusable. compound may or may not be present. resampling and reanalys cessary for verification.
c:tllll'med : -no..i11f;repla5ee~nec-ents-stitu-m oft-alchllllf' -l!!!!!I
Production Date: 11/14/97 07:34
METALS SAMPLE ANALYSIS
Sample 12430 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSO~ CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC011 SD
Media: SEDIM
RESULTS UNITS
0.74U MG/KG
2.6U MG/KG
93 MG/KG
0.91J MG/KG
037U MG/KG
12J MG/KG
39 MG/KG
23 MG/KG
16 MG/KG
11 MG/KG
1.8U MG/KG
1.8U MG/KG
2.2U MG/KG
52 MG/KG
42 MG/KG
0.17U MG/KG
18000 MG/KG
260 MG/KG
1100 MG/KG
2500 MG/KG
23000 MG/KG
200J MG/KG
1700 MG/KG
46 %
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: MJ02
D Number: MJ02
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org C'.lntractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
K-actual valu~is k wn to be less than value given. L-actual value is known to be greater than value-· n. U-material was analyzed for but not detected.
R-qc indicates t a unusable. compound may or may not be present. resampling and reanaJysi ssary for verification.
C1111if1ed" 1-no v-rep'llilee ca1e C"llilfnls -lituelillllllr'e of t'liill chl'lilll --
Production Date: 11/14/97 07:34
-
METALS SAMPLE ANALYSIS
Sample 12420 FY 1997
METALS SCAN
EPA-REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC012SW MD Number: MH92
Media: SURFACEWA
RESULTS
2U
7U
23
1U
1U
2U
29
9U
15J
3J
SU
SU
6U
1J
9U
0.20U
150U
330
5800
2400
1400
4700J
1300
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAO
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MH92
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 11 :12
Ending:
Production Date: 11/14/97 07:34
R..qc indicates_~~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv. U-rnaterial was analyzed for but not detected. the number 1s the minimum q;Jla on llm1t
C-c-ed b,._,, -oval-port-• chi-con-s 2 .• uentlil'ta tec'iliilithlor'lillll ------
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12421 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC012SD MD Number: MH93
Media: SEDIM D Number: MH93
RESULTS UNITS ANALYTE
0.60U MG/KG SILVER
2.1U MG/KG ARSENIC
140 MG/KG BARIUM
1.3J MG/KG BERYLLIUM
0.30U MG/KG CADMIUM
14J MG/KG COBALT
37 MG/KG CHROMIUM
17 MG/KG COPPER
15 MG/KG NICKEL
16 MG/KG LEAD
3U MG/KG ANTIMONY
1.5U MG/KG SELENIUM
3U MG/KG THALLIUM
56 MG/KG VANADIUM
69 MG/KG ZINC
0.14U MG/KG TOTAL MERCURY
25000 MG/KG ALUMINUM
470 MG/KG MANGANESE
730 MG/KG CALCIUM
4200 MG/KG MAGNESIUM
28000 MG/KG IRON
170J MG/KG SODIUM
3800 MG/KG POTASSIUM
35 % % MOISTURE
lnorg Contractor: CHEM
Ofg Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 11 :30
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-Presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value gil~material was analyzed for but not detected. the number 1s the minimum q;J/lant n 1tm1t
R-qc indicates !~:-unusable. compound may or may not be present. resampling and reanalysis is sary for verification.
C-c-dby ... w.val-port"l!lilchlc'jilil°ons-2.a,ent5Mtab techllW'lord-----Im -
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12431 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC013SW MD Number: MK06
Media: SURFACEWA D Number: MK06
RESULTS
2U
7U
22
1U
1U
2U
1U
4U
1U
2U
5U
5U
6U
1U
3U
0.20U
90U
37
5900
3000
360
4500J
1200
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
· UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A•average value. NA-not analyzed. NAl-inlerferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:35
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detect-ed. the num-ber is the m-inimum qu;ljnli · n 1-imit.
R-qc indicates t~~-unusable. compound may or may not be present. _resampling and reanalysis i~A.:ary for verification.
C-c~1111d by ..,.w11111111 val~ .. portellii chlo-cons-2.c.ents-ta~tech-lord. -
METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12432 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC013SD MD Number: MK07
Media: SEDIM
RESULTS
0.59U
2.1U
57
0.55J
0.29U
6.7J
16
11
7.3J
4.7
1.5U
1.5U
1.8U
22
20
0.13U
9400
360
550
1400
11000
130J
890
32
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MK07
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produce_d by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:50
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value giv~-material was analyzed for but not detected. the number is the minimum qu;lln · limit.
R-qc indicates that-unusable. compound may or may not be present. resampling and reanalysis is sary for verification.
C-co-d by ..,.w. valu-orte-chlor-onst-2.c.ents -•b ech,_lord... ------
METALS SAMPLE ANALYSIS
Sample 12419 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC014SW MD Number: MH91
Media: SURFACEWA D Number: MH91
RESULTS UNITS ANALYTE
2U UG/L SILVER
7U UG/L ARSENIC
50 UG/L BARIUM
1U UG/L BERYLLIUM
1U UG/L CADMIUM
2U UG/L COBALT
1U UG/L CHROMIUM
4U UG/L COPPER
1U UG/L NICKEL
2J UG/L LEAD
5U UG/L ANTIMONY
5U UG/L SELENIUM
6U UG/L THALLIUM
3J UG/L VANADIUM
20U UG/L ZINC
0.20U UG/L TOTAL MERCURY
380U UG/L ALUMINUM
140 UG/L MANGANESE
7300 UG/L CALCIUM
3300 UGIL MAGNESIUM
1300 UG/L IRON
4800J UG/L SODIUM
3200 UG/L POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:45
Ending:
Production Date: 11/14/97 07:34
R-qc indicates 1~:aunusable. compound may or may not be present. resampling and reanalysis i sary for verification.
K-actual value is known to be less than value given. L-actua1 value is known to be greater than value g~ive LI-material was analyzed for but not detected. the number 1s the minimum qu~nt n hm1t
C-c?liid by .,.w. valu-ortewchlor-onst-2 .• ents -•b ech ... lord... ----111!!1 -
METALS SAMPLE ANALYSIS
Sample 12418 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Stalion:JC014SD MD Number: MH90
Media: SEDIM D Number: MH90
RESULTS UNITS ANALYTE
1U MG/KG SILVER
4.5 MG/KG ARSENIC
230 MG/KG BARIUM
2.3 MG/KG BERYLLIUM
0.40U MG/KG CADMIUM
24 MG/KG COBALT
70 MG/KG CHROMIUM
30 MG/KG COPPER
32 MG/KG NICKEL
22 MG/KG LEAD
2.4J MG/KG ANTIMONY
2.3 MG/KG SELENIUM
5U MG/KG THALLIUM
80 MG/KG VANADIUM
84 MG/KG ZINC
0.23U MG/KG TOTAL MERCURY
34000 MG/KG ALUMINUM
950 MG/KG MANGANESE
3600 MG/KG CALCIUM
6800 MG/KG MAGNESIUM
37000 MG/KG IRON
270J MG/KG SODIUM
5000 MG/KG POTASSIUM
56 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:33
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAJ-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actuat value is known to be less than value given. L-actual value is known to be weater than valu~ ~iven. LI-material w~s a~alyzed for but not detected. the number is the minimum qu~nr · n limit.
R-qc indicates th-unusable. compound may or may not be present. resampling and reanalysis ,a::~ry for venficat1on.
C-confirmed by g .when no value is reportedj see chloriiilijonsti-2.constituents -a~echn-lorda--------. -
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12427 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC015SW MD Number: MH99
Media: SURFACEWA D Number: MH99
RESULTS
2U
7U
39
1U
1U
2U
1U
5U
1U
2U
5U
5U
6U
1J
6U
0.20U
300U
130
7200
3400
2700
3900J
1300
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 11 :47
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual_value is known to be less than value given. L-actual value is known to be weater than valu~ ~~iv LI-material w~~ a~alyzed for but not detected. the number 1s the mrn,mum qu;Jln n limit
R-qc indicates t~~-unusable. compound may or may not be present. resampling and reanalysis I sary for venf1cat1on.
C-confirmed by,,,,, .w. valu-porteilii chloiill°ons-2 .• enls-ta tech.,lord------1111
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12428 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC015SD MD Number: MJ00
Media: SEDIM D Number: MJ00
RESULTS UNITS ANALYTE
0.71 U MG/KG SILVER
2.5U MG/KG ARSENIC
110 MG/KG BARIUM
1.1J MG/KG BERYLLIUM
0.35U MG/KG CADMIUM
11J MG/KG. COBALT
33 MG/KG CHROMIUM
19 MG/KG COPPER
12J MG/KG NICKEL
18 MG/KG LEAD
1.8U MG/KG ANTIMONY
1.8U MG/KG SELENIUM
2.1U MG/KG THALLIUM
47 MG/KG VANADIUM
63 MG/KG ZINC
0.17U MG/KG TOTAL MERCURY
23000 MG/KG ALUMINUM
590 MG/KG MANGANESE
1200 MG/KG CALCIUM
2100 MG/KG MAGNESIUM
30000 MG/KG IRON
200J MG/KG SODIUM
1600 MG/KG POTASSIUM
45 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/9712:15
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~iv U-rnatericil was analyzed for but not detected. the number 1s the minimum qu;,,n n limit
R-qc indicates t~~-unusable. compound may or may not be present. resampling and reanalysis i sary for verification.
C-co-dby..,.w.valuiil'orte .. chlo-ons-2.c.ents-ab tech,.,lord----11!1 -
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12433 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC016SD MD Number: MK08
Media: SEDIM
RESULTS
0.92U
5U
180
2.1J
0.46U
17J
48
41
24
45
3J
2.3U
3.3J
98
82
0.29U
50000
760
1200
3200
40000
190J
2800
69
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG.
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MK08
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/9715:35
Ending:
Production Date: 11/14/97 07:34
R-qc indicates ~~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~ive. LI-material was analyzed for but not detected. the number 1s the m1n1mum q;flan n limit
C-confirmed by..,,.w. val-port ... chi-cons-2 .• ent .. ta tech-hlord----111!!11 --
METALS SAMPLE ANALYSIS
Sample 12425 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC017SW MD Number: MH97
Media: SURFACEWA
RESULTS
2U
7U
33
1U
1U
2U
6U au
4J
2U
5U
SU
6U
1J
SU
0.20U
160U
17
7800
3600
320
4300J
1200
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MH97
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:30
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number 1s the minimum qu;,,n n hm1t
R-qc indicates t~-unusable. compound may or may not be present. resampling and reanalysis i·s~ary for verification. C-co-r by.,. .wlllll value is reported, see chlor.const-2.constituents Mta ... tech .. lord. -----
METALS SAMPLE ANALYSIS
Sample 12426 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC017SD MD Number: MH98
Media: SEDIM D Number: MH98
RESULTS UNITS ANALYTE
0.78J MG/KG SILVER
1.9U MG/KG ARSENIC
42 MG/KG BARIUM
0.68J MG/KG BERYLLIUM
0.26U MG/KG CADMIUM
20 MG/KG COBALT
52 MG/KG CHROMIUM
15 MG/KG COPPER
10J MG/KG NICKEL
7.7 MG/KG LEAD
2U MG/KG ANTIMONY
1.3U MG/KG SELENIUM
1.6U MG/KG THALLIUM
70 MG/KG VANADIUM
18 MG/KG ZINC
0.12U MG/KG TOTAL MERCURY
10000 MG/KG ALUMINUM
820 MG/KG MANGANESE
580 MG/KG CALCIUM
680 MG/KG MAGNESIUM
22000 MG/KG IRON
110J MG/KG SODIUM
430 MG/KG POTASSIUM
24 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:40
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum qu~on limit
R-qc indicates t~ unusable. compound may or may not be present. resampling and reanalysis i-s~ary for verification.
C-co-dby.,1.w-valu .. ported,seechlo.const-2.constituentsiii{a-..techwlordllll 1111 -----
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12412 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC018SW MD Number: LL02
Media: SURFACEWA
RESULTS
2U
7U
26
1U
1U
1U
1U
SU
1U
4
SU
SU
6U
2U
40
0.20U
240U
300
6000
2500
2000
4400J
1400
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: LL02
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presurnptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 16:32
Ending:
Production Date: 11/14/97 07:34
R-qc indicates t~-unusable. compound may or may not be present. resamphng and reanalys1s I ssary for verification.
K-act~al value is known to be less than value given. L-actual value is known to be ~reater than valu~ ~~iv U-material w~s a~alyzed for but not detected. the number 1s the mm1mum qu;Jln n 1rm1t
C-e-0-d by,,,,, .w. val-porte .. chlo-onsw 2.c.ents-ta tech.,lord--1111 ----
METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12413 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC01 BSD MD Number: LL03
Media: SEDIM
RESULTS
0.79U
5.1
230
2.6
0.40U
22
63
42
27
47JN
3.2J
2.BJN
3J
110
130
0.27U
56000
630
1700
5000
44000
300J
4200
63
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: LL03
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith B11tes
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 17:35
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAJ-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~ive. U-material was analyzed for but not detected. the number 1s the minimum qu:,,nt n limit
R-qc indicates t~-unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-~-d by,.,. w-valuiiiportellii chic-cons-2.c.ents-ta 'tech.,lord-----..
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12414 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC019SD MD Number: LL04
Media: SEDIM D Number: LL04
RESULTS UNITS ANALYTE
0.80U MG/KG SILVER
4.4J MG/KG ARSENIC
200 MG/KG BARIUM
2.2 MG/KG BERYLLIUM
0.40U MG/KG CADMIUM
19J MG/KG COBALT
55 MG/KG CHROMIUM
33 MG/KG COPPER
24 MG/KG NICKEL
38 MG/KG LEAD
3.3J MG/KG ANTIMONY
3J MG/KG SELENIUM
2.8J MG/KG THALLIUM
94 MG/KG VANADIUM
110 MG/KG ZINC
0.21U MG/KG TOTAL MERCURY
49000 MG/KG ALUMINUM
530 MG/KG· MANGANESE
1500 MG/KG CALCIUM
4500 MG/KG MAGNESIUM
40000 MG/KG IRON
260J MG/KG SODIUM
3700 MG/KG POTASSIUM
57 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 17:50
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~·v U-material was analyzed for but not detected .. the number 1s the mmtmum qu":lln n limit
R-qc indicates I~--unusable. compound may or may not be present. resampling and reanalysis i ssary for verification.
C-c-d by~• .w. val-port._ chlo-cons-2 .• ents-ta techW'lord-1111!1 --liia --
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12415 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC020SW MD Number: LL05
Media: SURFACEWA
RESULTS
2U
7U
14
1U
1U
2U
1U
7U
1U
2U
5U
5U
6U
1U
26
0.20U
90U
45
5700
2300
180U
5000J
1600
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: LL05
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 15:00
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual_value is known to be less than value given. L-actual value is known to be ~reater than valu~ ~~iv U-material w~s a~alyzed for but not detected. the number 1s the minimum qu=-n n ttmit
R-qc indicates t~-unusable. compound may or may not be present. resamphng and reanalysis I ssary for venficat1on.
C-coad by,.,, .w. valu-portellllii chloiliiiil°ons-2 .• ents-ta tech~lord--Eal -EI\I --
METALS SAMPLE ANALYSIS
Sample 12416 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC021SW MD Number: LL06
Media: SURFACEWA
RESULTS
2U
7U
24
1U
1U
2U
1U
SU
1U
4J
SU
SU
6U
2U
20U
0.20U
180U
150
7200
2800
1200
6800J
1800
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM·
VANADIUM
ZINC
D Number: LL06
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 17:00
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual _value is known to be less than value given. L-actual value is known to be weater than valu~ ~cive. U-material w~s a~alyzed for but not detected. the number 1s the m1mmum qu;,,n n limit
R-qc indicates t~ unusable. compound may or may not be present. resamphng and reanalysis I ssary for venficatron. C-coait by taf' .wi;.. valu-orteilliii chic-cons-2.c.ents-a tech-lord------
METALS SAMPLE ANALYSIS
Sample 12417 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97 -0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC021SD MD Number: MH89
Media: SEDIM D Number: MH89
RESULTS UNITS ANALYTE
0.94J MG/KG SILVER
4.9 MG/KG ARSENIC
270 MG/KG BARIUM
2.2 MG/KG BERYLLIUM
0.40U MG/KG CADMIUM
24 MG/KG COBALT
62 MG/KG CHROMIUM
47 MG/KG COPPER
30 MG/KG NICKEL
46JN MG/KG LEAD
4J MG/KG ANTIMONY
2U MG/KG SELENIUM
4U MG/KG THALLIUM
100 MG/KG VANADIUM
130 MG/KG ZINC
0.25U MG/KG TOTAL MERCURY
66000 MG/KG ALUMINUM
490 MG/KG MANGANESE
1400 MG/KG CALCIUM
5100 MG/KG MAGNESIUM
64000 MG/KG IRON
350J MG/KG SODIUM
4300 MG/KG POTASSIUM
62 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 18:40
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g~·v Li-material was analyzed for but not detected. the number 1s the minimum qu;,,n hmit
R-qc indicates t~a-unusable. compound may or may not be present. resampling and reanalysis jc sary for verification.
C-co-dbyill'w-valu-orteillillchlo~ns-2.c ... nts-ab tech~lord--IIBI -BIi --
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12457 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC001 PW MD Number: MP68
Media: GROUNDWA
RESULTS
2U
7U
31
1U
1U
2U
1U
490
1U
11
5U
5U
6U
1U
100
0.20U
50U
BJ
2300
1300
30U
3000J
890
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MP68
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COM PU
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:15
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value g-ive U-material was analyzed for but not detected. the number 1s the minimum qu;Jlnr n limit
R-qc indicates t~a-unusable. compound may or may not be present. resampling and reanalysis i"' sary for verification.
C-co-d by ,,.,.w. val-porte .. chlo-consw 2 .• ents-ta tech.,lord-------
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12458 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC002PW MD Number: MP69
Media: GROUNDWA
RESULTS
2U
7U
8
1U
1U
2U
1U
20U
1U
2U
SU
SU
6U
1J
26
0.20U
40U
1U
11000
4700 sou
4900J
1300
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MP69
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 21 :00
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actuat value is known to be greater than value given. U-material was analyzed for but not detecte-d. the num-ber is the m-inimum qu;Jjnti · n Ii-mil. R-qc indicates t~-unusable. compound may or may not be present. resampling and reanalysis is·~~ry for verification. C-co-d by ..,.wh .. value is reporte .. chlor._.constituents 2.c11111ents ~ab~ech-lordllli. --
I
It
I
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
I
MEMORANDUM
I Date: 09/16/97
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I Subject: Results of METALS INORGANIC Sample Analysis
97-0329 JOHNSON CONTROLS GLOBE
I
I
I
From:
To:
WINSTON-SALEM, NC
Gary Bennett{¥~ -
PAT DEROSA
RECEIVED
SEP 19 1997,
SUPERFUND SECTION
Ached are the results of analysis of samples collected as part of the subject project. If you have any
g';stions, please contact me.
I
I
I
tTTACHMENT
I
I
It
I
II
I
.... INORGANIC DATA QUALIFIERS REPORT
.Case Number: Johnson Control Globe
I Project Number: 97-0329
Site: Johnson Control Globe, Winston-Salem, NC
I
I
I
I
I
I
I
I
I
I
I
Element
A. Soils
Sb, Cd, Pb, Se,
Ag
Ba
Be
Cd
Pb
Tl
Sb
As
Ba
Be
Cd
Cr
Cc
Cu
Pb
It
I
I
Flag
u
u
JN
JN
JN
J
J
J
R
J
J
J
J
J
J
J
Samples Affected
All positives >IDL, but< CRDL
< CRDL
All positives > IDL, ·but < CRDL
12476, 12479, 12480, 12481, 12482,
12483, 12484
12476, 12479, 12480, 12481, 12482.
12483, 12484, 12485
12476, 12477, 12478, 12479, 12480,
12481, 12482, 12483, 12484, 12485
12476, 12479, 12480, 12481, 12482,
12483, 12484
12476, 12477, 12478, 12479, 12480,
12481, 12482, 12483, 12484, 12485
12476, 12477, 12478, 12480, 12481,
12482, 12483, 12485
12479, 12484
12476, 12477, 12478, 12479, 12480,
12481, 12482, 12483, 12484, 12485
12476, 12477, 12478, 12479, 12480,
12481, 12482, 12483, 12484, 12485
Reason
Baseline instability
Positives in blanks
suspected positive interference
as noted in the contractor res
suspected positive interference
as noted in the coritractor res
suspected positive.interference
as noted in the contractor ICS
suspected over correction as
noted in the contractor res
Matrix spike recovery= 50.2%
Matrix spike recovery= 137.8%
Blind spike recovery< action
limit
Matrix spike recovery= 154.9%
Blind spike recovery< warning
limit
Matrix spike recovery 154.9%
Blind spike recovery > action
limit
12476, 12477, 12478, 12479, 12480, Matrix spike recovery= 161.2% 12481, 12482, 12483, 12484, 12485
12476, 12477, 12478, 12479, 12480, Matrix spiked recovery 159.2% 12481, 12482, 12483, 12484, 12485
12476, 12477, 12478, 12479, 12480,
12481, 12482, 12483, 12484, 12485
12476, 12477, 12478, 12479, 12480,
12481, 12482, 12483, 12484, 12485
12476, 12477, 12478, 12479, 12480,
12481, 12482, 12483, 12484, 12485
Matrix spike recovery= 152.2%
Blind spike recovery< action
lirni t
MatriX spike recovery 147.4%
Blind ·spike recovery< action
limit
Matrix spike recovery= 136.2%
Blind spike recovery < action
lirni t
serial dilution percent
difference= 11.1%
I
-Case
INORGANIC DATA QUALIFIERS REPORT (Continued)
Nwnber: Johnson Control Globe
I Project Number: 97-0329
Site: Johnson Control Globe, Winston-Salem, NC
Element Flag Samgles Affected Reason
I Ni J 12476, 12477, 124 7 8, 12479, 12480, Matrix spike recovery = 160%
12481, 12482, 12483, 12484, 12485
Ag J 12476, 12477, 124 78, 124 79, 12480, Matrix spike recovery 152.5% I 12481, 12482, 12483, 12484, 12485
V J 12476, 12477, 12478, 12 4 7 9, 12480, Matrix spike recovery= 163%
12481, 12482, 12483, 12484, 12485 Blind spike recovery< action I limit
Matrix spike Zn J 124 7 6, 12477, 12478, 12479, 12480, recovery= 148.8%
12481, 12482, 12483, 12484, 12485 Blind spike recovery< action I limit
Seril dilution percent
difference= 19.5%
I Al J 124 7 6, 12477, 12478, 12 4 7 9, 12480, Blind spike recovery < action 12481, 12482, 12483, 12484, 12485 limit
Seril dilution percent
I difference = 19.5%
Ca J 1247 6, 12477, 12478, 12479, 12480,. Blind spike recovery < action , 12481, 12482, 12483, 12 4 8 4, 12485 limit
Seril dilution percent
difference= 15.8%
Fe J 124 76, 12477, 124 78, 12479, 12480, Blind spike recovery < action I 12481, 12482, 12483, 12 4 8 4, 12485 limit
Seril dilution percent
difference= 15.7%
I Mg J 12476, 12477, 12478, 12 4 7 9, 124 BO, Blind spike recovery < warning
12481, 12482, 1,2483, 12484,-12485 limit
Seril dilution percent
I I difference= 17.2%
Mn J 12476, 12477, 12478, 12479, 12480, Blind spike recovery < action
12481, 12482, 12483, 12484, 12485 limit
I -Seril dilution percent
difference= 16.8%
K J 12476, 12477, 12478, 12 4 7 9, 12480, Blind spike recovery < action
I 12 4 81, 12482, 1248 3, 12484, 12485 limit
As u 124 77, 12485 % RSD > 20% for ICP multiple
exposures and results were> I IDL, but < CRDL
Hg J 12476, 12477, 12478, 12479, 12480, No instrument printout of data
'-12481, 12482, 12483, 12484, 12485 included in raw data
I
I
I
INORGANIC DATA QUALIFIERS REPORT (Continued)
Nwnber: Johnson Control Globe
Project Nurnber:~9~7~--=03~2~9c_ ____________ _
Site: Johnson Control Globe, Winston-Salem, NC
Element
I TCLP Extract
Pb,
I Ba
I
I
I
I ,,
I
I
I
I
ii
II
'-I
I
Se
Cr
Cr
Pb
. As
Cd
Se
Ag
Cc.
Cr
Se
Ag
As
As
Ba
Flag
u
u
J
J
J
u
u
u
u
J
J
J
J
J
J
J
Samples Affected
All positives> IDL, but
< CRDL
All positives> IDL, but
< l0X ~ontaminant level
12476, 12477, 12478, 12479,
12481, 12482, 12483, 12484,
12476, 12477, 12478, 12479,
12481, 12482, 12483, 12484,
12476, 12477, 12478, 12479,
12 4 81, 12482, 12483, 12484,
12476, 12477
12476, 12477, 12478
12481, 12484
12481, 12483, 12485
12482, 12483, 12484
12480
12485
12480
12485
12480,
12485
12479, 12481, 12482, 12483, 12484
12476, 12478, ·12.480, 12485
12480, 12484
12479, 12480
12477, 12478, 12479, 12480, 12481
12483, 12484, 12485
12476, 12477, 12478, 12479, 12480
12481, 12482, 12483, 12484, 12485
Reason
Baseline instability
Positives in blanks
Negative with absolute value>
CRDL reported in blank
Matrix duplicate RPO= 200%
Serial dilution percent
difference= 12.7%
% RSD > 20% for ICP multiple
exposures and results > IDL,
but< CRDL
% RSD > 20% foe ICP multiple
exposures and results > IDL,
but< CRDL
% RSD > 20% for ICP multiple
exposures and results > IDL,
but< CRDL
% RSD > 20% for ICP multiple
exposures and results > IDL,
but< CRDL
% RSD > 2 0% for ICP multiple
exposures
% RSD > 20% for ICP multiple
exposures
·% RSD > 21n-for ICP multiple
exposures
% RSD > 20% for ICP multiple
exposures
Only analysis of
standard required by
SOW for ICP analysis
2X CRDL
contract
No extraction blank analyzed by
the laboratory
No extraction blank analyzed by
the laboratory
I
ltcase
I
INORGANIC DATA QUALIFIERS REPORT (Continued)
I
I
I
I
I
I
I
I
I
I
I
Number: Johnson Control Globe
Project Number:_,9~7~-~0~3~2,e.s,9 _____________ _
Site: Johnson Control Globe, Winston-Salem, NC
Element Flag Samples Affected
Cd J 12477, 12478, 12479, 12480,
12482, 124 83, 12484, 12485
Cr J 12477, 12478, 12479, 12480,
12482, 12483, 12484
Pb J 12476, 12477, 12478, 12479,
12481, 12482, 12483, 12484,
Se J 12476, 12478, 12480, 12481,
12484, 12485
It
I
I
Reason
12481 No extraction blank
the laboratory
12481 No extraction blank
the laboratory
12480 No extraction blank
12485 the laboratory
12483 No extraction blank
the laboratory
analyzed by
analyzed by
analyzed by
analyzed by
N-"-!IIS -- -
Sample. 12476 FY 1997 Project: 97--0329
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB010SL MD Number: MP65
Media: SOIL
RESULTS
13000J
0.6UJ
0.96J
100J
0.85J
4.1JN
1100J
32J
18J
20J
19000J
26JN
2500J
760J
0.34J
19J
2200J
0.32U
2.6J
54
0.36UJ
51J
370J
23
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
--Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 17:20
Ending:
-iWr
A-average value. NA-not analyzed. NAl-lnterferences. J-estimated v·alue. N-presumptive evidence of presence of material.
K-actual va_lue is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitatlon limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constitlients or metabolites of technical chlordane
-ET~ lliillA --ON
Sample 12476 FY 1997 Project: 97-0329
METALS TCLP SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB01 0SL
Media: SOIL
RESULTS
0.007U
0.007U
1.6J
NA
0.003U
0.01UJ
NA
0.022J
NA
0.00BJ
NA
0.0002U
UNITS
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
MD Number: MP65
TOTAL MERCURY
SAS Number:TCLP
lnorg Contractor: ANTEC
--Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 17:20
Ending:
-
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanatysls is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technic.al chlordane
-ET~ ANAl!!illl IS ---Sample 12477 FY 1997
METALS SCAN
Project: 97-0329
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB001 SL
Media: SOIL
RESULTS UNITS
6200J MG/KG
0.58UJ MG/KG
1UJ MG/KG
53J MG/KG
0.57J MG/KG
2.3J MG/KG
490J MG/KG
20J MG/KG
9.8J MG/KG
14J MG/KG
8700J MG/KG
16JN MG/KG
1600J MG/KG
210J MG/KG
0.08UJ MG/KG
10J MG/KG
1000J MG/KG
0.31U MG/KG
2.3J MG/KG
46 MG/KG
0.36U MG/KG
25J MG/KG
32J MG/KG
14 %
MD Number: MP70
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
--Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 17: 15
Ending:
-
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value Is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
11619,,,41
AN..,IS--Sample 12477 FY 1997
METALS TCLP SCAN
Project: 97-0329 -IIIIIA--ON
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB001 SL
Media: SOIL
RESULTS
0.007U
0.008UJ
0.98J
NA
0.00SUJ
0.012J
NA
0.012J
NA
0.003U
NA
0.0002U
UNITS
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
MD Number: MP70
TOTAL MERCURY
SAS Number:TCLP
lnorg Contractor: ANTEC
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
---Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 17:15
Ending:
-
K-actual v~lue is known to be less than value given. L-actual value Is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-ET,-AN/lllalS --Sample 12478 FY 1997
METALS TCLP SCAN
Project: 97 -0329
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
ld/Station:JB101SL MD Number: MP71 lnorg Contractor: ANTEC
Media: SOIL
RESULTS
0.007U
0.76J
0.92J
NA
0.003UJ
0.025J
NA
0.025J
NA
0.011J
NA
0.0002U
UNITS
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
TOTAL MERCURY
--Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 17: 15
Ending:
-
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of preserlce of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R..qc Indicates that data unusable. compound may or may not be present. resampling and reanalysls is necessary for verification.
C--confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constltuents or metabolites of technical chlordane
-ET~ AN.slll!S al -Sample 12478 FY 1997 Project: 97-0329
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB101SL MD Number: MP71
Media: SOIL
RESULTS
6000J
0.64UJ
0.84J
65J
0.61J
2.2J
640J
19J
10J
15J
8400J
19JN
1600J
370J
0.12UJ
9.7J
1000J
0.34U
2.1J
38
0.39U
25J
30J
15
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
--Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 17:15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-ET .... --Sample 12479 FY 1997
METALS SCAN
Project: 97--0329
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB003SL
Media: SOIL
RESULTS UNITS
7500J MG/KG
0.59UJ MG/KG
0.49UR MG/KG
53J MG/KG
0.69JN MG/KG
3.4JN MG/KG
1600J MG/KG
26J MG/KG
10J MG/KG
21J MG/KG
16000J MG/KG
7.3JN MG/KG
4200J MG/KG
370J MG/KG
0.09UJ MG/KG
16J MG/KG
1800J MG/KG
0.32U MG/KG
2.7J MG/KG
370 MG/KG
0.36UJ MG/KG
47J MG/KG
52J MG/KG
14 %
MD Number: MP72
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
--Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 18:30
Ending:
-
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence or material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no va"tue is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-ET,_ AN .... IS --Sample 12479 FY 1997
METALS TCLP SCAN
Project: 97 -0329 -lliillA --ON D~EN..,.. ---Printed by: Ron Phelps
Collected By:
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC Beginning: 08/13/97 18:30
Ending: Program: NSF
ld/Station:JB003SL MD Number: MP72
Media: SOIL
RESULTS
O.OO?U
0.006J
0.20J
NA
0.004UJ
0.014J
NA
O.OOBJ
NA
0.003U
NA
0.0002U
UNITS
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
TOTAL MERCURY
SAS Number:TCLP
lnorg Contractor: ANTEC
-lllllllh
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value Is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-ET~ AN ... IS ---Sample 12480 FY 1997 Project: 97-0329
METALS TCLP SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JB004SL
Media: SOIL
MD Number: MP73
RESULTS
0.012J
0.009J
2.0J
NA
0.009J
0.03J
NA
0.074J
NA
0.007J
NA
0.0002U
UNITS
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
TOTAL MERCURY
SAS Number:TCLP
lnorg Contractor: ANTEC
--Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 17:45
Ending:
-
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituentS or metabolites of technical chlordane
~T.lal
Sample 12480 FY 1997
METALS SCAN
--Project: 97-0329
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF .
ld/Station:JB004SL MD Number: MP73
Media: SOIL
RESULTS
13000J
0.51 UJ
1.3J
83J
0.99J
4.1JN
1200J
27J
13J
29J
20000J
74JN
3100J
650J
0.11 UJ
19J
2100J
0.27U
2.6J
97
0.31 UJ
53J
100J
7
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM-
ZINC
% MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
- -
Printed by: Ron Phelps
Collected By:
Beginning:_08/13/97 17:45
Ending:
-8r
A-average value. NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. ·
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
ANJIIIIIIIS --..,_flllloN
Sample 12481 FY 1997 Project: 97.()329
METALS TCLP SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JB005SL
Media: SOIL
RESULTS
0.01UJ
0.013J
1.03J
NA
0.007J
0.018J
NA
0.012J
NA
0.004UJ
NA
0.0002U
UNITS
MG/L
MG/L
MGIL
MG/L
MGIL
MG/L
MG/L
MGIL
MG/L
MG/L
MGIL
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
MD Number: MP74
TOTAL MERCURY
SAS Number:TCLP
lnorg Contractor: ANTEC
--Printed by: Ron Phelps
Collected By:
Beginning: 08/13197 19:00
Ending:
-
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value Is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis Is necessary for verification.
C-confirmed by gems: 1.when no value Is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
a1ET~ --Sample 12481 FY 1997 Project: 97--0329
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB00SSL
Media: SOIL
RESULTS UNITS
14000J MG/KG
0.52UJ MG/KG
1.SJ MG/KG
76J MG/KG
0.64JN MG/KG
4.2JN MG/KG
4500J MG/KG
28J MG/KG
8.8J MG/KG
27J MG/KG
20000J MG/KG
18JN MG/KG
3300J MG/KG
270J MG/KG
0.11 UJ MG/KG
14J MG/KG
2900J MG/KG
0.28U MG/KG
2.4J MG/KG
98 MG/KG
0.32UJ MG/KG
52J MG/KG
54J MG/KG
12 %
MD Number: MP74
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
--Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 19:00
Ending:
-
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be preseht. resampllng and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-ET,_ -Sample 12482 FY 1997 Project: 97-0329
METALS TCLP SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JB006SL
Media: SOIL
MD Number: MP75
RESULTS
0.00?U
0.005U
1.2J
NA
0.012J
0.012J
NA
7.1J
NA
0.003U
NA
0.0002U
UNITS
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
TOTAL MERCURY
SAS Number:TCLP
lnorg Contractor: ANTEC
--Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 19:00
Ending:
-
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actuaf value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see--chlordane constituents 2.constituents or metabolites of technical chlordane
-=TJ!allA N.ial!IS --Sample 12482 FY 1997
METALS SCAN
Project: 97 -0329 -
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB006SL MD Number: MP75
Media: SOIL
RESULTS UNITS ANALYTE
15000J MG/KG ALUMINUM
0.78UJ MG/KG ANTIMONY
2.2J MG/KG ARSENIC
82J MG/KG BARIUM
0.95JN MG/KG BERYLLIUM
5.3JN MG/KG CADMIUM
4700J MG/KG CALCIUM
36J MG/KG CHROMIUM
14J MG/KG COBALT
62J MG/KG COPPER
26000J MG/KG IRON
2000JN MG/KG LEAD
3500J MG/KG MAGNESIUM
510J MG/KG MANGANESE
0.15UJ MG/KG TOTAL MERCURY
23J MG/KG NICKEL
2300J MG/KG POTASSIUM
0.42U MG/KG SELENIUM
3.5J MG/KG SILVER
820 MG/KG SODIUM
0.47UJ MG/KG THALLIUM
68J MG/KG VANADIUM
180J MG/KG ZINC
38 % % MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
--Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 19:00
Ending:
-!WT
•
A-average value. NA-not analyzed. NAl-interferences. J-estlmated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actuar value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
ANIIIIIIS ---Sample 12483 FY 1997
METALS SCAN
Project: 97 -0329
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JB007SL
Media: SOIL
RESULTS UNITS
17000J MG/KG
0.61UJ MG/KG
1.9J MG/KG
88J MG/KG
0.83JN MG/KG
5.2JN MG/KG
1200J MG/KG
43J MG/KG
13J MG/KG
27J MG/KG
24000J MG/KG
1000JN MG/KG
3200J MG/KG
650J MG/KG
0.13UJ MG/KG
25J MG/KG
3100J MG/KG
0.33U MG/KG
2.9J MG/KG
70 MG/KG
0.38UJ MG/KG
54J MG/KG
110J MG/KG
21 %
MD Number: MP76
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
--Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 20:30
Ending:
-
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantltation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12483 FY 1997 Project: 97-0329
METALS TCLP SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JB007SL
Media: SOIL
MD Number: MP76
RESULTS
0.008UJ
0.08J
1.23J
NA
0.008J
0.019J
NA
4.8J
NA
O.OOBJ
NA
0.0002U
UNITS
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
TOTAL MERCURY
SAS Number:TCLP
lnorg Contractor: ANTEC
--Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 20:30
Ending:
-8r
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-ET,_ AN/llilalS ---Sample 12484 FY 1997
METALS TCLP SCAN
Project: 97-0329
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JB008SL
Media: SOIL
RESULTS
0.012J
0.018J
1.35J
NA
0.006J
0.011J
NA
0.19J
NA
0.005UJ
NA
0.0002U
UNITS
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
MD Number: MP77
TOTAL MERCURY
DN
SAS Number:TCLP
lnorg Contractor: ANTEC
--Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 20:35
Ending:
-
A-average value. NA-not analyzed. N~l-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual varue is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
~T/Wl9A N/11111S---Sample 12484 FY 1997 Project: 97-0329
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE
Program: NSF
WINSTON-SALEM, NC
Id/Station: JB008SL MD Number: MP77
Media: SOIL
RESULTS UNITS ANALYTE
13000J MG/KG ALUMINUM
0.64UJ MG/KG ANTIMONY
0.53UR MG/KG ARSENIC
130J MG/KG BARIUM
1JN MG/KG BERYLLIUM
4.5JN MG/KG CADMIUM
710J MG/KG CALCIUM
27J MG/KG CHROMIUM
14J MG/KG COBALT
27J MG/KG COPPER
21000J MG/KG IRON
68JN MG/KG LEAD
4100J MG/KG MAGNESIUM
1000J MG/KG MANGANESE
0.14UJ MG/KG TOTAL MERCURY
23J MG/KG NICKEL
4800J MG/KG POTASSIUM
0.34U MG/KG SELENIUM
4.2J MG/KG SILVER
76 MG/KG SODIUM
0.39UJ MG/KG THALLIUM
45J MG/KG VANADIUM
77J MG/KG ZINC
28 % % MOISTURE
i>N
SAS Number:TCLP
lnorg Contractor: ANTEC
--Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 20:35
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
C
Sample 12485 FY 1997
METALS TCLP SCAN
-Project: 97 -0329 -
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB009SL MD Number: MP78
Media: SOIL
RESULTS
0.009UJ
0.011J
1.6J
NA
0.007J
0.01U
NA
0.56J
NA
0.01J
NA
0.0002U
UNITS
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
TOTAL MERCURY
SAS Number:TCLP
lnorg Contractor: ANTEC
--Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 21 :45
Ending:
-
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
C
AN .... IS--Sample 12485 FY 1997
METALS SCAN
Project: 97-0329
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB009SL
Media: SOIL
RESULTS
7500J
1UJ
1UJ
87J
0.54J
2.7JN
960J
16J
9.6J
20J
12000J
49JN
2600J
710J
0.07UJ
15J
2800J
0.31U
1.7J
58
0.35U
26J
71J
8
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
MD Number: MP78
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
- -Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 21:45
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence or presence or material.
K-actual value Is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane con_stituents 2.constituents or metabolites of technical chlordane