NCD000770487_19980728_Johnson Controls Battery Group_FRBCERCLA SAP QAPP_Sample Analysis 1997 - 1998-OCR

• •
UNITED STA TES ENVIRONMENTAL PROTECTION AGENCY
REGION 4
July 28, 1998
Mr. Doug Moore
SCIENCE AND ECOSYSTEM SUPPORT DIVISION
OFFICE OF QUALITY ASSURANCE
980 COLLEGE STATION RD
A THENS, GA 30605-2720
I
JUL ii l l::i::18
SUPEH1-u1~u .:it:GTION
North Carolina Department of Health, Environment and Natural Resources
Superfund Section
401 Oberlan Road, Suite 150
Raleigh, North Carolina
Dear Mr Moore:
Enclosed is the inorganic and organic forms that you requested for Johnson Control Globe,
case no. 25633, project no. 97-378.
If you have any questions or if I may be of further assistance, please contact me at 706/355-
8622.
Sincerely,
Diane A. Guthrie, P.E.
Environmental Engineer
Enclosure
. . . i •
a. Syste1n Monitofir1g Co1npou11d Summary
' (For1n II V{)A)
J5035
q7/ o3Jg
· "'LL Ci~ 51)& . v
22
all 2A • WATER VOLATw; SYSTEM MONITORING COMPOUND COVERY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Contract: 68D50004
SAS No.: SDG No. : DLL02
page OJ... o.f 0 1
EPA SMCl SMC2 SMC3 OTHER TOT
SAMPLE NO. (TOL) # (BFB)# (DCE)# OUT
------------====== ====== ===:::c== ===::::== 01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
VBLKMM
DMH91
DMH92
DMH94
VBLKTG
DMH95
DMH97
DMH99
DMJ0l
DMK06
VBLKXG
DMK09
DMKll
DMK13
DMP51
DMP52
DMP57
DMP59
DMP61
DMK13MS
DMK13MSD
VBLKYY
DLL02
DLL05
DLL06
VBLKQA
VHBLKG7
SMCl
SMC2
SMC3
(TOL)
(BFB)
(DCE)
---
102 100 95 0
102 102 98 0
109 108 105 0
98 96 95 0
105 104 100 0
104 104 99 0
102 101 100 0
105 104 102 0
107 108 105 0
109 109 104 0
104 100 97 0
102 100 98 0
102 100 100 0
96 94 94 0
102 99 98 0
104 102 102 0
105 102 102 0
103 100 103 0
105 102 102 0
95 93 99 0
101 96 107 0
89 86 84 0
91 90 88 0
89 88 85 0
89 88 86 0
100 98 95 0
97 96 93 0
--
--
--
Toluene-dB
Bromofluorobenzene
l,2-Dichloroethane-d4
QC LIMITS
(88-110)
(86-115)
(76-114)
# Column to be used to flag recovery values
* Values outside of contract required QC limits
FORM II VOA-1 OLM03.0
23
•
a. Surrogate Percent Recovery Summary
~;f-(Form II SV)
285
all 2C • WATER smvoLATILE SURROGATE RECOVERY
Lab Name: CompuChem Env. Corp.
Lab Code: COMPO Case No. : 25633
Contract: 68D50004
SAS No.: SDG No. : DLL02
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
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25
26
27
28
29
30
EPA Sl S2 S3 S4 S5 S6 S7 SB TOT ~PLE NO. (NBZ) # (FBP)# (TPH)# (PHL)# (2FP) # (TBP) # (2CP) # (DCB)# OUT ------------====== ====== ====== ====== ====== ====== ====== ====== === SBLKTG 66 64 87 72 77 76 76 56 0 DMH91 65 66 117 67 63 95 68 49 0 DMH95 72 72 100 72 74 86 80 58 0 DMH97 60 61 91 65 63 76 68 52 0 DMH99 67 68 94 72 74 81 77 64 0 DMJ0l 64 65 93 68 67 79 74 54 0 DMK06 62 63 85 67 67 75 72 53 0 DMK09 36 34* 44 36 34 41 37 28 l DMH92 78 81 117 85 86 98 90 68 0 DMKll 79 81 113 84 74 95 90 66 0 DLL05 61 66 98 65 65 76 70 49 0 DLL06 68 65 106 67 71 82 73 52 0 DLL02 62 62 99 62 59 75 69 50 0 DMH94 73 80 95 80 83 78 83 64 0 SBLKTH 47 49 111 52 55 76 54 39 0 DMK13 71 80 103 84 83 90 86 64 0 DMK13MS 69 71 111 72 67 94 74 54 0 DMK13MSD 70 74 113 84 80 99 86 60 0 DMP52 87 84 112 86 93 98 95 76 0 DMP57 61 66. 105 72 68 91 73 55 0 DMP51 87 92 112 97 98 106 101 78 0 DMP61 81 85 120 87 88 90 93 71 0 DMP59 83 85 126 88 88 100 93 72 0
-
-
-
-
-
' . -1-----
I ____
~-" QC LIMITS
Sl (NBZ) Nitrobenzene-d5 (35-114)
S2 (FBP) 2-Fluorobiphenyl (43-116)
S3 (TPH) Terphenyl-dl4 (33-141)
S4 (PHL) Phenol-d5 (10-110)
S5 (2FP) = 2-Fluorophenol (21-110)
S6 (TBP) 2,4,6-Tribromophenol (10-123)
S7 (2CP) 2-Chlorophenol-d4 (33-110) (advisory)
S8 (DCB) l,2-Dichlorobenzene-d4 (16-110) (advisory)
# Colunm to be used to flag recovery values
* Values outside of contract required QC limits
D Surrogate diluted out
page OT:o"f 01 FORM II SV-1 OLM03.0
286
•
a. Sys_te1n Mo11itori.:1g Co1npou11d Summary
(F or111 II \'()A)
22 ·
SOIL VOLAT. SYSTE~
8
MONITORING COMPOUND .OVERY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU
Level: (low/med) LOW
Case No. : 25633
Contract: 68050004
SAS No.: SDG No.: DMP60
page OJ.: of 01
EPA SMCl SMC2 SMC3 OTHER TOT
SAMPLE NO. (TOL) # (BFB)# (DCE)# OUT
------------====== ====:::::= ====== =====:::;: ---
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
VBLKX3
DMP64 .
DMP70
DMP71
DMP72
DMP74
DMP75
DMP64MS
VBLKYl
DMP65
DMP66
DMP67
DMP73
DMP64MSD
VBLKW6
DMP60
DMP62
DMP77
DMP78
DMP81
VBLKDl
DMP76
VBLKLl
VHBLKX3
SMCl
SMC2
SMC3
(TOL) =
(BFB) =
(DCE) =
86 83 83 0
101 105 110 0
92 84 92 0
92 86 95 0
87 100 98 0
96 107 117 0
97 101 113 0
88 96 101 0
96 89 105 0
102 94 106 0
96 88 103 0
104 97 110 0
98 90 105 0
108 110 117 0
87 83 92 0
100 95 108 0
98 92 106 0
104 99 110 0
94 92 106 0
104 100 115 0
92 86 97 0
93 90 102 0
100 91 100 0
102 92 102 0
--
--
--
--
--
--
Toluene-dB
Bromofluorobenzene
l,2-Dichloroethane-d4
QC LIMITS
(84-138)
(59-113)
(70-121)
tt Column to be used to flag recovery values
* Values outside of contract required QC limits
FORM II VOA-2 OLM03.0
23
•·
a. Surrogate Percent Recovery Summary-
(Form II SV)
;)_:0R3 3
. z q1 ✓ o3J
DfYlpei,o
346
SOIL
2D
SE.OLATILE SURROGATE
Lab Name: COMPUCHEM ENV. CORP.
RECOVERY •
Lab Code: COMPU
Level: (low/med) LOW
Case No. : 25633
Contract: 68D50004
SAS No.: SDG No . : BMP6D
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
EPA Sl S2 S3 S4 S5 S6 S7 S8
SAMPLE NO. (NBZ) # (FBP)# (TPH) # (PHL) # (2FP) # (TBP) # ( 2CP) # (DCB)#
------------==:::=== =====::;: ;;::::::::::::== ::::::;::;;::;;::;::;; ::;::;:::;;::;;:;:::;; ====== ====== ::;;::;;::;:::;;::;;::;:
SBLKRS 26 26* 33 25 21* 26 26 24
DMP64 57 49 61 53 53 51 54 50
DMP64MS 50 49 52 49 49 46 ·51 46
DMP64MSD 53 49 58 50 50 46 52 47
DMP65 52 50 60 48 47 52 48 44
DMP72 32 32 36 31 28 29 29 26
SBLKRR 56 53 70 53 52 49 54 50
DMP60 53 51 60 53 51 50 53 45
DMP62.. . 51 50 57 50 50 47 5l.."' • 44 ., .
DMP65RE 47 46 61 45 45 · 51 45 43
DMP67 39 35 53 36 36 43 36 35
DMP70 36 32 44 34 34 38 34 33
DMP75 30 28* 33 29 28 29 29 27
DMP76 40 36 38 38 38 37 39 36
DMP77 44 40 54 41 40 35 42 41
DMP78 28 25* 36 27 26 29 27 26
DMP76DL 29 26D 31 29 28 24 28 26
SBLKZV 52 47 65 51 47 48 51 44
DMP66 67 61 78 66 62 55 66 55
DMP73 49 43 53 48 48 45 49 40
DMP74 32 29* 54 32 29 42 30 24
SBLKAG 46 39 75 42 42 44 42 37
DMP71 54 47 62 54 54 54 56 39
Sl (NBZ) Nitro'benzene-d5
QC LIMITS
(23-120)
S2 (FBP) 2-Fluorobiphenyl (30-115)
S3 (TPH) Terphenyl-dl4 (18-137)
S4 (PHL) = Phenol-d5 (24-113)
S5 (2FP) 2-Fluorophenol (25-121)
S6 (TBP) = 2,4,6-Tribromophenol · (19-122)
S7 (2CP) 2-Chlorophenol-d4 (20-130) (advisory)
S8 (DCB) l,2-Dichlorobenzene-d4 (20-130) (advts-FY)
# Column to be used to flag recovery values
* Values outside of contract required QC limits
D Surrogate diluted out
TOT
OUT
---
2
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
1
0
0
-
-
--
--
-
--
-
page 01 of 01 FORM II SV-2 OLM03.0
347
,
' '
•
a. System Monitoring Compound Su1n1nary
(F or1n II V() A)
21
• 2A •
WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No.: 25633
Contract: 68D50004
SAS No.: SDG No. : DMP63
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
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23
24
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26
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29
EPA
SAMPLE NO.
------------
VBLK.XG
DMP63
DMP68
DMP69
VBLKTA
DMP80
VBLKYY
DMP79
DMP79MS
DMP79MSD
DMP98
VBLKTJ
VHBLKV5
SMCl
(TOL)#
======
104
105
100
103
110
106
89
89
88
89
93
106
110
SMC2 SMC3 OTHER TOT
(BFB)# (DCE)# OUT
====== ====== ====== ---
100 97 0
103 103 0
98 102 0
100 104 0
107 113 0
104 107 0
86 84 0
87 85 0
87 86 0
90 84 0
93 86 0
104 100 0
110 107 0
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--~ -. 30
page 01 of 01
SMCl
SMC2
SMC3
(TOL)
(BFB)
(DCE) ~
Toluene-dB
Bromofluorobenzene
l,2-Dichloroethane-d4
--
QC LIMITS
(88-110)
( 86-115)
(76-114)
# Column to be used to flag recovery values
* Values outside of contract required QC limits
FORM II VOA-1 OLM03.0
22·
•
I i
a. Sys_tem Monitoring Compound Summary
(For1n II VC>A)
c)s-033
q_7_,03;),?
D L-L,03
~:
38
• 2B •
SOIL VOLATILE SYSTEM MONITORING COMPOUND R!"coVERY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU
Level: (low/med) LOW
Case No.: 25633
Contract: 68D50004
SAS No.: SDG No. : DLL03
~ i
~ "
page 01 of 01
EPA SMCl SMC2 SMC3 OTHER TOT
SAMPLE NO. (TOL)# (BFB)# (DCE)# OUT
------------====== ====== ====== ====== ---
01 VBLKV9•
02 DMH89
03 DMH90
04 DMH93
05 DMH96
06 DMH98
07 DMJ00
08 DMJ02
09 DMK07
10 DMK0S
11 DMKl0
12 DMH89MS
13 DMH89MSD
14 VBLKW5
15 DMK12
16 DMK14
17 DMP50
18 DMP53
19 DMP54
20 DMP55
21 VBLKW6
22 DMP56
23 DMP58
24 DLL03
25 DLL04
26 VHBLKXl
27
28
29
30
SMCl
SMC2
SMC3
(TOL)
(BFB)
(DCE) =
102 93 100 0
100 88 99 0
100 91 103 0
103 95 105 0
102 91 99 0
102 93 106 0
101 93 104 0
106 100 111 0
104' 99 110 0
105 97 106 0
102 96 106 0
111 104 102 0
109 104 104 0
98 93 107 0
100 91 106 0
104 103 107 0
100 95 106 0
96 92 109 0
92 89 101 0
99 96 109 0
87 83 92 0
102 96 110 0
110 104 113 0
104 99 114 0
100 91 105 0
95 92 106 0
--
--
--
--
Toluene-dB
Bromofluorobenzene
l,2-Dichloroethane-d4
QC LIMITS
(84-138)
(59-113)
(70-121)
.
# Column to be used to flag recovery values
* Values outside of contract required QC limits
FORM II VOA-2 OLM03.0
39
•
a. Surrogate Percent Recovery Summary
J: i. (Form II SV)
-: ....
349
A 2D •
SOIL SEM~LATILE SURROGATE RECOVERY
Lab Name: COMPUCHEM ENV. CORP."
Lab Code: COMPU
Level: (low/med) LOW
Case No. : 25633
Contract: 68D50004
SAS No.: SDG No. : DLL03
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
EPA 81 82 83 84 85 86 87 88
~!>LE NO. (NBZ) # (FBP)# (TPH) # (PHL)# (2FP) # (TBP) # (2CP) # (DCB)#
------------====== ====== ====== ====== ====== ====== ====== ;;;:::::::::::::;;::::
SBLKRQ 41 38 44 39 40 40 40 36
DMH89 37 37 44 36 34 43 35 31
DMH89MS 46 47 56 46 46 54 46 40
DMH89MSD 49 45 46 46 48 46 48 42
DMH90 40 38 44 39 37 42 38 34
DMH93 50 47 50 48 48 46 49 44
DMH96 38 38 40 38 39 40 39 33
DMJ02 42 42 48 44 42 48 43 36
DMK07 61 60 63 62 67 47 65 54
DMK08 55 53 53 54 57 52 57 48
DMKl0 55 53 54 55 58 52 57 47
DMK12 55 54 56 55 59 51 58 49
DMK14 33 32 44 32 32 42 32 29
DMP50 55 56 .. 60 56 57 60 57 48
DMP53 36 34 44 36 36 40 36 32
DMP54 41 43 49 44 42 50 43 34
DMH98 51 51 55 48 53 46 52 44
DMJ00 41 44 50 40 40 49 41 37
DMP55 49 49 47 48 50 50 51 43
SBLKRS 26 26* 33 25 21* 26 26 24
DMP55DL 56 55 62 54 51 56 55 47
SBLKRR 56 53 70 53 52 49 54 50
DMP58 48 48 62 47 44 48 46 40
DMP56 66 65 79 68 66 60 70 58
DLL04 31 28* 33 29 28 30 29 26
SBLKAG 46 39 75 42 42 44 42 37
DLL03 66 58 78 68 72 70 72 53
-. -
QC LIMITS
81 (NBZ) Nitrobenzene-d5 (23-120)
82 (FBP) = 2-Fluorobiphenyl (30-115)
83 (TPH) Terphenyl-dl4 (18-137)
84 (PHL) Phenol-d5 (24-113)
85 (2FP) = 2-Fluorophenol (25-121)
86 (TBP) = 2,4,b-Tribromophenol (19-122)
87 (2CP) 2-Chlorophenol-d4 (20-130) (advisory)
88 (DCB) = l,2-Dichlorobenzene-d4 (20-130) (advisory)
# Column to be used to flag recovery values
* Values outside of contract required QC limits
D Surrogate diluted out
TOT
OUT
---
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
0
0
1
0
0
--
--
-
page 01 of 01 FORM II SV-2 OLM03.0
350
b. Matrix Spike/Jvlitrix Spik:e Duplicate
· Stn11r."Jary
~, (For1n III VOA_)
24
•
3A A
WATER VOLATILE MA X SPIKE/MATRIX SPIKE DUPLI<:.a RECOVERY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No.: 25633
Contract: 68D50004
SAS No.: SDG No. : DLL02
Matrix Spike -EPA Sample No.: DMK13
SPIKE SAMPLE MS MS ADDED CONCENTRATION CONCENTRATION % COMPOUND (ug/L) (ug/L) (ug/L) REC # ------------------------========= ==========::::::::::: ============= ====::;:::: 1,1-Dichloroethene 50.00 0.000 53.48 107 Trichloroethene 50.00 0.000 49. 31 99 Benzene 50.00 0.000 51.98 104 Toluene 50.00 0.000 49.12 98 Chlorobenzene 50.00 0.000 47.26 94
SPIKE MSD MSD
QC.
. LIMITS
REC.
======
61-145
71-120
76-127
76-125
75-130
ADDED CONCENTRATION e-0 % QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. -===========--====----=----------============= ===:=== ====== ====== =====:::: 1,1-Dichloroethene 50.00 56.51 113 5 14 Trichloroethene 50.00 51.02 102 3 14 Benzene 50.00 53.05 106 2 11 Toluene 50.00 50.33 101 3 13 Chlorobenzene 50.00 48.83 98 4 13
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: 0 out of
Spike Recovery:
COMMENTS:
5 outside limits
0 out of 10 outside limits
FORM III VOA-1
61-145
71-120
76-127
76-125
75-130
OLM03.0
25
b. Matrix Spike/Matrix Spike Duplicate
Summary
~;t-(Form III SV)
287
ft 3C A WATER SEMIVOLATILE .,RIX SPIKE/MATRIX SPIKE DUPL~TE RECOVERY
Lab Name: CompuChem Env. Corp.
Lab Code: COMPU Case No. : 25633
Matrix Spike -EPA Sample No.: DMK13
SPIKE
coM'tofum ADDED
(ug/L)
---------------------------------Phenol 75.00
2-Chlorophenol 75.00
1,4-Dichlorobenzene 50.00
N-Nitroso-di-n-prop. (1) 50.00 1,2,4-Trichlorobenzene 50.00 4-Chloro-3-methylphenol 75.00 Acenaphthene 50.00 4 -Nit rophenol 75.00 2;4-Dinitrotoluene 50.00
Pentachlorophenol 75.00 Pyrene 50.00
SPIKE
Contract: 68D50004
SAS No.: SDG No. : DLL02
SAMPLE MS MS CONCENTRATION CONCENTRATION ,._
0 (ug/L) (ug/L) REC # =---==---==--=--====::::::::::::::;:::;;:::::::::: =====::;:
0.000 55.06 73
0.000 52.30 70 0.000 33.32 67
0.000 34.92 70 0.000 37.28 74 0.000 58.93 78
0.000 43.48 87 0.000 63.30 84• 0.000 40.24 80 0.000 85.96 115* 0.000 54.39 109
MSD MSD
QC.
LIMITS
REC.
:::::::;:::::===
12-110
27-123
36-97
41-116
39-98
23-97
46-118
10-80
24-96
9-103
26-127
ADDED CONCENTRATION %-,._
0 QC LIMITS COMPOUND (ug/L) (ug/L) REC j/ RPD # RPD REC. ----------------------------------------------:::;;:::;;::;;:::;:::::;; ====== ===::::::::::::; ====== Phenol 75.00 63.11 84 14 42 2-Chlorophenol 75.00 61.03 81 14 40 1,4-Dichlorobenzene 50.00 38.28 76_ 12 28 N-Nitroso-di-n-prop. (1) 50.00 37.26 74 6 38 1,2,4-Trichlorobenzene 50.00 40.34 81 9 28 4-Chloro-3-methylphenol 75.00 63.81 85 8 42 Acenaphthene 50.00 46.10 92 6 31 4-Nitrophenol 75.00 87.51 117* 33 50 2,4-Dinitrotoluene 50.00 44. 96 90 12 . 38 Pentachlorophenol 75.00 99.40 132* 14 -50 Pyrer,e " 50.00 53.48 107 2 31
(1) N-Nitroso-di-n-propylamine
# Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits
RPD: O out of 11 outside limits Spike Recovery: 4 out of 22 outside limits
COMMENTS:
FORM III SV-1
12-110
27-123
36-97
41-116
39-98
23-97
46-118
10-80
24-96
9-103
26-127
OLM03.0
288
b. Matrix Spike/Matrix Spik:e Duplicate
S u1111?1ary
~ ,f (Form III V01~-)
24
A 3B • SOIL VOLATILE MAT~ SPIKE/MATRIX SPIKE DUPLICA RECOVERY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Contract: 68D50004
SAS No.: SDG No.: DMP60
Matrix Spike -EPA Sample No.: DMP64 Level: (low/med) LOW
SPIKE SAMPLE MS MS
ADDED CONCENTRATION CONCENTRATION %
COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC #
-----------------------------------------------------------======== 1,1-Dichloroethene 65.79 0.000 40.82 62
Trichloroethene 65.79 0.000 44.97 68
Benzene 65.79 0.000 48.01 73
Toluene 65.79 0.000 40.71 62
Chlorobenzene 65.79 0.000 40.46 61
SPIKE MSD MSD
QC.
LIMITS
REC.
======
59-172
62-137
66-142
59-139
60-133
ADDED CONCENTRATION % % QC LIMITS
COMPOUND (ug/Kg) (ug/Kg) REC # RPD # RPD
----------------------------------------------====== ====== ======
1,1-Dichloroethene 65.79 56.74 86 32* 22
Trichloroethene 65.79 74 .49 113 50* 24
Benzene 65.79 76.47 116 46* 21
Toluene 65.79 68.92 105 51* 21
Chlorobenzene 65.79 69.46 106 54* 21
# Column .t:-o be used to flag recovery and RPD values with an asterisk
~ "
• Values outside of QC limits
RPD: 5 out of 5 outside limits
Spike Recovery: O out of 10 outside limits
COMMENTS:
-: -
FORM III VOA-2
REC.
======
59-172
62-137
66-142
59-139
60-133
OLM03.0
25
•
b. Matrix Spike/Matrix Spike Duplicate,_
Summary
(Form III S V)
348
3D
SOIL SEMIVOLATILE .RIX SPIKE/MATRIX SPIKE DUPL.TE RECOVERY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Matrix Spike -EPA Sample No.: DMP64
SPIKE
ADDED
COMPOUND (ug/Kg)
---------------------------------Phenol ' 3289
2-Chlorophenol 3289
1,4-Dichlorobenzene 2193
N-Nitroso-di-n-prop. (1) 2193
1,2,4-Trichlorobenzene 2193
4-Chloro-3-methylphenol 3289
Acenaphthene 2193
4-Nitrophenol 3289
2,4-Dinitrotoluene 2193
Pentachlorophenol 3289
Pyrene 2193
SPIKE
Contract: 68D50004
SAS No.: SDG No. : BM?-60
Level: (low/med) LOW
SAMPLE MS MS
CONCENTRATION CONCENTRATION %
(ug/Kg) (ug/Kg) REC #
------------- -------------::::=====
0.000 1526 46
0.000 1543 47.
0.000 1109 50
0.000 1054 48
0.000 1170 53
0.000 1546 47
0.000 1172 53
0.000 1642 " ~o -0.000 1211 55
0.000 1126 34
0.000 1177 54
MSD MSD
QC.
LIMITS
REC.
======
26-90
25-102
28-104
41-126
38-107
26-103
31-137
11-114
28-89
17-109
35-142
ADDED CONCENTRATION % % QC LIMITS
COMPOUND (ug/Kg) (ug/Kg) REC # RPD # RPD REC.
----------------------------~,-,;----------------====== ====== ====== ::;:::;::::;::;::::;::;:::;:
Phenol 3289 1528 46 0 35
2-Chlorophenol 3289 1536 47 0 50
1,4-Dichlorobenzene 2193 1132 52 4 27
N-Nitroso-di-n-prop. (1) 2193 1059 48 0 38
1,2,4-Trichlorobenzene 2193 1164 53 0 23
4-Chloro-3-methylphenol 3289 1569 48 2 33
Acenaphthene 2193 1174 54 2 19
4-Nitrophenol 3289 1680 51 2 50
2,4-Dinitrotoluene 2193 1280 58 5 47
Pentachlorophenol 3289 711.4 22 43 47
Pyrene 2193 1324 60 10 36
(1) N-Nitroso-di-n-propylamine
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: 0 out of 11 outside limits
Spike Recovery: O out of 22 outside limits
COMMENTS:
FORM III SV-2
26-90
1 25-102
28-104
41-126
38-107
26-103
31-137
11-114
28-89
17-109
35-142
OLM03.0
349
•
b. Matrix Spike/Metrix Spil(e Duplicate
s lllTilY:_ary
J: ., -(F or1n III VO A,)
-= ....
23
• 3A
WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE • DUPLICATE RECOVERY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Matrix Spike -EPA Sample No.: DMP79
SPIKE
ADDED
COMPOUND (ug/L)
---------------------------------1,1-Dichloroethene 50.00
Trichloroethene 50.00
Benzene 50.00
Toluene 50.00
Chlorobenzene 50.00
SPIKE
Contract: 68D50004
SAS No.: SDG No. : DMP63
SAMPLE MS MS
CONCENTRATION CONCENTRATION ,,_
0
(ug/L) (ug/L) REC # --------------------------======
0.000 45.31 91
0.000 43.90 88
0.000 44.14 88
0.000 43.73 87
0.000 43.48 87
MSD MSD
QC.
LIMITS
REC.
==::;===
61-145
71-120
76-127
76-125
75-130
ADDED CONCENTRATION ,,_
0
,,_
0 QC LIMITS
COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC.
----------------------------------------------====== ====== ====== ======
1,1-Dichloroethene 50.00 46.09 92 1 14
Trichloroethene 50.00 45.55 91 3 14
Benzene 50.00 45.76 92 4 11
Toluene 50.00 45.20 90 3 13
Chlorobenzene 50.00 44.35 89 2 13
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: O out of
Spike Recovery:
COMMENTS:
5 outside limits
O out of 10 outside limits
FORM III VOA-1
61-145
71-120
76-127
76-125
75-130
OLM03.0
24
•
b. Matrix Spik:e/M,3.trix Spil(e Duplicate
S u1nr:1.ary
~ ,-(Form III V01\)
40
• 3B
SOIL VOLATILE MATRIX SPIKE/MATRIX • SPIKE DUPLICATE RECOVERY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPO Case No.: 25633
Matrix Spike -EPA Sample No.: DMH89
SPIKE
ADDED
COMPOUND (ug/Kg)
---------------------------------
1,1-Dichloroethene 122.0
Trichloroethene 122.0
Benzene 122.0
Toluene 122.0
Chlorobenzene 122.0
SPIKE
Contract: 68D50004
SAS No.: SDG No. : DLL03
Level: (low/med) WW
SAMPLE MS MS
CONCENTRATION CONCENTRATION %
(ug/Kg) (ug/Kg) REC #
--------------------------======
0.000 114.0 93
0.000 116.1 95
0.000 126.5 104
0.000 121. 0 99
0.000 114.6 94
MSD MSD
QC.
LIMITS
REC.
=====:::
59-172
62-137
66-142
59-139
60-133
ADDED CONCENTRATION % % QC LIMITS
COMPOUND (ug/Kg) (ug/Kg) REC # RPD # RPD REC.
----------------------------------------------====== ::;:;:;:;;:;:;:;:;:;:;:;: ====== ======
1,1-Dichloroethene 122.0 123.8 101 8 22
Trichloroethene 122.0 119.6 98 3 24
Benzene 122.0 127.1 104 0 21
Toluene 122.0 123.8 101 2 21
Chlorobenzene 122.0 115.8 95 1 21
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: 0 out of 5 outside limits
Spike Recovery: O out of 10 outside limits
COMMENTS:
FORM III VOA-2
59-172
62-137
66-142
59-139
60-133
OLM03.0
41
•
b. Matrix Spike/Matrix Spike Duplicate
Summary
J: .. -(Form III SV) .
351
A 3D A
SOIL SEMIVOLATILE MA'MIX SPIKE/MATRIX SPIKE DUPLI~E RECOVERY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No.: 2,5,633
Contract: 68D50004
SAS No.: SDG No. : DLL03
Matrix Spike -EPA Sample No.: DMH89 Level: (low/med) LOW
-SPIKE SAMPLE MS MS
.J: i ADDED CONCENTRATION CONCENTRATION %
COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC #
======================== -----------------------------------====:;:::=
Phenol 6098 0.000 2655 44
2-Chlorophenol 6098 0.000 2546 42
1,4-Dichlorobenzene 4065 0.000 1781 44
N-Nitroso-di-n-prop. (1) 4065 0.000 1938 48
1,2,4-Trichlorobenzene 4065 0.000 1904 47
4-Chloro-3-methylphenol 6098 0.000 3342 55
Acenaphthene 4065 0.000 2284 56
4-Nitrophenol 6098 0.000 3420 56
2,4-Dinitrotoluene 4065 0.000 2462 60
Pentachlorophenol 6098 0.000 2248 37
Pyrene 4065 0.000 2365 58
SPIKB MSD MSD
QC.
LIMITS
REC.
======
26-90
25-102
28-104
41-126
38-107
26-103
31-137
11-114
28-89
17-109
35-142
ADDED CONCENTRATION % ,._
0 QC LIMITS
COMPOUND (ug/Kg} (ug/Kg} REC # RPD # RPD
----------------------------------------------====== ====== ======
Phenol 6077 2683 44 0 35
2-Chlorophenol 6077 2676 44 5 50
1,4-Dichlorobenzene 4052 1916 47 6 27
N-Nitroso-di-n-prop. (1) 4052 2020 50 4 38
1,2,4-Trichlorobenzene 4052 1994 49 4 23
4-Chloro-3-methylphenol 6077 2895 48 14 33
Acenaphthene 4052 2026 50 11 19
4-Nitrophenol 6077 3172 52 7 50
2,4-Dinitrotoluene 4052 2179 54 10 47
Pentachlorophenol 6077 1636 27 31 . -47
Pyrene " 4052 2023 50 15 36
(1) N-Nitroso-di-n-propylamine
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: O out of 11 outside limits
Spike Recovery: O out of 22 ouJ:_side limits
COMMENTS:
--·-
FORM III SV-2
REC.
======
26-90
25-102
28-104
41-126
38-107
26-103
31-137
11-114
28-89
17-109
35-142
OLM03.0
352
• •
c. Method Blank: S'urn1nary (For111 IV VOA)
If n1ore than a single fonn is necessary, fonns shall
be arranged in clu·o'.~ological order by date of
analysis of the blanlc, and by instnnnent.
26
4a 4A
VOLATJ91l METHOD BLANK SUMMARY • EPA SAMPLE NO.
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No.: 25633
Lab File ID: CB970818C55
Date Analyzed: 08/18/97
GC Col~:-DB624
Instrument ID: F50055
ID: 0. 53 (mm)
Contract: 68D50004
SAS No.:
VBLKMM
SDG No. : DLL02
Lab Sample ID: VBLKMM
Time Analyzed: 0659
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
6-2
•· "'£3
COMMENTS:
24
25
26
27
28
29
30
page 01 Qf 91
EPA
SAMPLE NO.
------------
DMH91
DMH92
DMH94
LAB
SAMPLE ID
--------------
864 726
864733
864734
LAB TIME
FILE ID ANALYZED
------------------------CN064'726A55 1241
CN064733A55 1321
CN064734A55 1400
-
FORM IV VOA OLM03.0
· 27
i:a 4A
VOLAT:Na' METHOD BLANK SUMMARY • EPA SAMPLE NO.
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: CB970821B55
Date Analyzed: 08/21/97
GC Col~:-DB624
Instrument ID: F50055
ID: O. 53 (mm)
Contract: 68D50004
SAS No.:
VBLKTG
SDG No. : DLL02
Lab Sample ID: VBLKTG
Time Analyzed: 2044
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
-· "23
COMMENTS:
24
25
26
27
28
29
30
page 01 .9J _01
EPA
SAMPLE NO.
------------
DMH95
DMH97
DMH99
DMJ0l
DMK06
LAB
SAMPLE ID
--------------
864735
864736
864 738
864 739
864740
LAB TIME
FILE ID ANALYZED
------------------------CN064735B55 0426
CN064736B55 0505
CN064738B55 0544
CN064739B55 0623
CN064740B55 0703
. -
FORM IV VOA OLM03.0
28
•
4A
VOLAT METHOD BLANK SUMMARY • EPA SAMPLE NO.
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: CB970822A55
Date Analyzed: 08/22/97
GC CollrnI.i: DB624
Instrument ID: F50055
ID: 0. 53 (mm)
Contract: 68D50004
SAS No.:
VBLKXG
SDG No. : DLL02
Lab Sample ID: VBLKXG
Time Analyzed: 0856
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
~-'23
24
25
26
27
28
29
30
COMMENTS:
page 01 EJ _01
EPA
SAMPLE NO.
------------
DMK09
DMKll
DMK13
DMP51
DMP52
DMP57
DMP59
DMP61
DMK13MS
DMK13MSD
LAB
SAMPLE ID
===========:::::::::::::::
864741
864 742
864 743
864744
864745
864746
864747
864748
864727
864728
LAB TIME
FILE ID ANALYZED
==-====-====-= ----------
CN064741A55 1024
CN064742A55 1113
CN064743A55 1146
CN064744A55 1220
CN064745A55 1255
CN064746A55 1336
CN064 74 7A55 1416
CN064748A55 1451
CN064727A55 1741
CN064728A55 1825
.
. -
FORM IV VOA OLM03.0
29
a 4A
VOLAT:Ur METHOD BLANK SUMMARY • EPA SAMPLE NO .
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: CB970823A55
Date Analyzed: 08/23/97
GC Col~: DB624
Instrument ID: F50055
ID: O. 53 (mm)
Contract: 68D50004
SAS No.:
VBLK.YY
SDG No. : DLL02
Lab Sample ID: VBLKYY
Time Analyzed: 0704
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
i22 ~·· ""23
COMMENTS:
24
25
26
27
28
29
30
page 01...Qf_0l
EPA
SAMPLE NO.
------------
DLL02
DLL05
DLL06
LAB
SAMPLE ID
===========:::::-=
864761
864762
864 763
LAB TIME
FILE ID ANALYZED
------------------------CR064761A55 0840
CR064762A55 0918
CR064763A55 0956
. -
FORM IV VOA OLM03.0
30
4A
VOLAT. METHOD BLANK SUMMARY • EPA SAMPLE NO .
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: CB970902A55
Date Analyzed: 09/02/97
GC Colunm: DB624 J, i.
Instrument ID: F50055
ID: 0. 53 (mm)
Contract: 68D50004
SAS No.:
VBLKQA
SDG No. : DLL02
Lab Sample ID: VBLKQA
Time Analyzed: 0841
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
2.2
_., -Q3
COMMENTS:
24
25
26
27
28
29
30
page 01 of 01
EPA
SAMPLE NO.
=======-===-
VHBLKG7
LAB
SAMPLE ID
=============:::;
864730
.
LAB TIME
FILE ID ANALYZED
============== ----------CN064730A55 1059
-
FORM IV VOA OLM03.0
31
• •
c. Method Blank Summary (Form IV SV)
I{ :.tmore than a single form is necessary, forms shall be
arranged in chronological order by date of analysis and by
instrument. ·
289
A 4B • EPA SAMPLE NO. SEMI~TILE METHOD BLANK SUMMARY
Lab Name: CompuChem Env. Corp.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH065194A60
Instrument ID: 5972HP60
Matrix.). Jsoil/water) WATER
Level: (low/med) LOW
Contract: 68D50004
SAS No.:
SBLKTG
SDG No. : DLL02
Lab Sample ID: 865194
Date Extracted: 08/18/97
Date Analyzed: 08/24/97
Time Analyzed: 0910
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
-· -72 23
COMMENTS:
24
25
26
27
28
29
30
page 01 of e1
EPA
SAMPLE NO.
------------
DMH91
DMH95
DMH97
DMH99
DMJ0l
DMK06
DMK09
DMH92
DMKll
DLL05
DLL06
DLL02
DMH94
LAB
SAMPLE ID
==========::;===
864 726
864735
864 736
864 738
864739
864740
864 741
864733
864 742
864762
864763
864761
864 734
LAB DATE
FILE ID ANALYZED
------------------------GH064726A60 08/24/97
GH064735A60 08/24/97
GH064736A60 08/24/97
GH064 738A60 08/24/97
GH064739A60 08/24/97
GH064740A60 08/24/97
GH064741A60 08/24/97
GH064733A60 08/24/97
GH064 742B60 08/24/97
GH064762B60 08/24/97
GH064 763B60 08/24/97
GH064761B60 08/25/97
GJ064734A60 08/25/97
. -
FORM IV SV-1 OLM03.0
290
QI. 4B • EPA SAMPLE NO. SEMIV~ILE METHOD BLANK SUMMARY
Lab Name: CompuChem Env. Corp.
Lab Code: COMPU Case No.: 25633
Lab File ID: GH065196A60
Instrument ID: 5972HP60
Matrix J, its·oil/water) WATER
Level: (low/med) LOW
Contract: 68D50004
SAS No.:
SBLKTH
'
SDG No. : DLL02
Lab Sample ID: 865196
Date Extracted: 08/19/97
Date Analyzed: 08/25/97
Time Analyzed: 1827
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
~ ~ 23
24
25
26
27
28
29
30
COMMENTS:
page 01 at e1
EPA
SAMPLE NO.
------------
DMK13
DMK13MS
DMK13MSD
DMP52
DMP57
DMP51
DMP61
DMP59
LAB
SAMPLE ID
--------------
864743
864 731
864732
864745
864746
864 744
864 748
864 74 7
LAB DATE
FILE ID ANALYZED
--------------=-====::====
GH064743A60 08/25/97
GH064731A60 08/25/97
GH064732A60 08/25/97
GH064745A60 08/25/97
GH064746A60 08/25/97
GH064744A60 08/26/97
GH064748C60 08/26/97
GH064747C60 08/26/97
. -
FORM IV SV-1 OLM03.0
291
•
c. Method Blanl( Slnnmary (For1n IV VOA)
If 111ore than a sing1<: form is necessary, forn1s shall
be arranged in chrc,nological order by date of
analysis of the blarb:: and by instrun1ent.
26:
'
A 4A
VOLATIDMETHOD BLANK SUMMARY • EPA SAMPLE NO.
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH064803B51
Date Analyzed: 08/20/97
GC Col~ -DB624
Instrument ID: F50051
ID: 0.53 (mm)
Contract: 68D50004
SAS No.:
VBLKX3
SDG No. : DMP60
Lab Sample ID: 864803
Time Analyzed: 2245
Heated Purge: (Y/N) Y
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
:Z-2 .. 23
COMMENTS:
24
25
26
27
28
29
30
page 01 .,;;f JJl
EPA
SAMPLE NO.
========:==:cc:=
DMP64
DMP70
DMP71
DMP72
DMP74
DMP75
DMP64MS
LAB
SAMPLE ID
--------------
864 704
864714
864715
864716
864718
864719
864705
LAB TIME
FILE ID ANALYZED
=====:;:::======== ----------
GH064704B51 2344
GH064714B51 0217
GH064715B51 0254
GH064716B51 0330
GH064718B51 0442
GH064719B51 0518
GH064705B51 0554
. -
FORM IV VOA OLM03.0
27
& 4A • EPA SAMPLE NO.
VOLATI .. METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH065763A52
Date Analyzed: 08/21/97
GC Col~J DB624
Instrument ID: F50052
ID: 0.53 (mm)
Contract: 68D50004
SAS No.:
VBLKYl
SDG No. : DMP60
Lab Sample ID: 865763
Time Analyzed: 0756
Heated Purge: (Y/N) Y
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
2-2
-· ~3
24
25
26
27
28
29
30
COMMENTS:
page 01 ..af .Dl
EPA
SAMPLE NO.
------------
DMP65
DMP66
DMP67
DMP73
DMP64MSD
LAB
SAMPLE ID
--------------
864 711
864 712
864713
864 717
864706
LAB TIME
FILE ID ANALYZED
------------------------GR064711A52 112'3
GR064712A52 1211
GR064713A52 1322
GR064717A52 1359
GR064706A52 1433
. -
FORM IV VOA OLM03.0
28
ah 4A
VOLATIJlrMETHOD BLANK SUMMARY • EPA SAMPLE NO.
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH064795B52
Date Analyzed: 08/21/97
GC Col~i DB624
Instrument ID: F50052
ID: O. 53 (mm)
Contract: 68D50004
SAS No.:
VBLKW6
SDG No.: DMP60
Lab Sample ID: 864795
Time Analyzed: 1853
Heated Purge: (Y/N) Y
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
EPA LAB LAB TIME
SAMPLE NO. SAMPLE ID FILE ID ANALYZED
--------------------------============== ----------
01 DMP60 864702 'GH064 702B52 2157
02 DMP62 864703 GH064703B52 2239
03 DMP77 864721 GH064721B52 2359
04 DMP78 864 722 GH064722B52 0045
05 DMP81 864723 GH064723B52 0123
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21 . :z.2 . -
23
24
25
26
27
28
29
30
COMMENTS:
page 01 ~f -01
FORM IV VOA OLM03.0
29
4ii1' 4A
VOLATM METHOD BLANK SUMMARY • EPA SAMPLE NO.
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH065474B52
Date Analyzed: 08/22/97
GC Colu.J111,r DB624
Instrument ID: F50052
ID: 0. 53 (mm)
Contract: 68D50004
SAS No.:
VBLKDl
SDG No.: DMP60
Lab Sample ID: 865474
Time Analyzed: 1907
Heated Purge: (Y/N) Y
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
z-2 .• 23
COMMENTS:
24
25
26
27
28
29
30
page O 1 ..o,f ./l l
EPA
SAMPLE NO.
------------DMP76
LAB
SAMPLE ID
==============
864720
LAB TIME
FILE ID ANALYZED
========----------------G2R64720B52 2052
-
FORM IV VOA OLM03.0
30
A 4A
VOLATM METHOD BLANK SUMMARY • EPA SAMPLE NO.
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH066220B52
Date Analyzed: 08/24/97
GC Col~ DB624
Instrument ID: F50052
ID: O. 53 (mm)
Contract: 68D50004
SAS No.:
VBLKLl
SDG No. : DMP60
Lab Sample ID: 866220
Time Analyzed: 2010
Heated Purge: (Y/N) Y
THIS METHOD BLANK APPLIES TO THE FOLWWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
2-2 ~ ~3
COMMENTS:
24
25
26
27
28
29
30
page 01 ..of _01
EPA
SAMPLE NO.
------------
VHBLKX3
LAB
SAMPLE ID
--------------
864707
LAB TIME
FILE ID ANALYZED
------------------------GH064707B52 0306
-
FORM IV VOA OLM03.0
31
• •
c. Method Blank Summary (Form IV S\7)
If more than a single form is necessary, forms shall be
arranged in chronological order by date of analysis and by
instrument.
350
4B EPA SAMPLE NO.
SEMIV.ILE METHOD BLANK SUMMARY •
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPO Case No. : 25633
Lab File ID: GJ064768A66
Instrument ID: 5972HP66
Matrix: (soil/water) SOIL
Level: (low/med) LOW
Contract: 68D50004
SAS No.:
SBLKRS
SDG No . : BMP6-D
Lab Sample ID: 864768
Date Extracted: 08/15/97
Date Analyzed: 09/17/97
Time Analyzed: 1428
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD
COMMENTS:
-01-
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
page 01 of 01
EPA
SAMPLE NO.
------------
DMP64
DMP64MS
DMP64MSD
DMP65
DMP72
DMP65RE
DMP67
DMP70
DMP75
DMP76
DMP77
DMP78
DMP76DL
LAB LAB DATE
SAMPLE ID FILE ID ANALYZED ------------------------------------------------864 704'' GH064704A66 09/17/97
864709 GH064709A66 09/17/97
864710 GH064710A66 09/17/97
864 711 GH064711A66 09/17/97
864716 GH064716A66 09/17/97
864711 GJ064711A66 09/18/97
864713 GJ064713A66 09/18/97
864714 GH064714A66 09/18/97
864719 GH064719A66 09/18/97
864 720 GH064720A66 09/18/97
864721 GH064721A66 09/18/97
864722 GH064722A66 09/18/97
864720 GD064720A66 09/19/97
••
FORM IV SV-1 OLM03.0
351
4B
SEMIV.TILE METHOD
EPA SAMPLE NO .
BLANK SUMMARY • Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No.: 25633
Lab File ID: GJ064766A66
Instrument ID: 5972HP66
Matrix: (soil/water) SOIL '•
Level: (low/med) LOW
SBLKRR
Contract: 68D50004
SAS No.: SDG No.: BM1l6-0
Lab Sample ID: 864766
Date Extracted: 08/15/97
Date Analyzed: 09/18/97
Time Analyzed: 1117
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD
COMMENTS:
0L
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
page 01 of 01
EPA
SAMPLE NO.
------------
DMP60
DMP62
LAB
SAMPLE ID
--------------864702
864 703
LAB DATE
FILE ID ANALYZED
----------~ -------------------------
GJ064702A66 09/18/97
GJ064703A66 09/18/97
FORM IV SV-1 OLM03.0
352
4B
SEMIV.TILE METI'(()D
EPA SAMPLE NO.
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH068696A66
Instrument ID: 5972HP66
Matrix: (soil/water) SOIL
Level: (low/med) LOW
BLANK SUMMARY • Contract: 68D50004
SAS No.:
SBLKZV
SDG No . : 8M!l6{)
Lab Sample ID: 868696
Date Extracted: 09/18/97
Date Analyzed: 09/20/97
Time Analyzed: 1226
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD
COMMENTS:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
page 01 of 01
EPA
SAMPLE NO.
------------
DMP66
DMP73
DMP74
LAB
SAMPLE ID
--------------
864712
864717
864 718''
.•
LAB DATE
FILE ID ANALYZED
----------~ ------------------------
GR064712A66 09/20/97
GR064717A66 09/20/97
GR064718A66 09/20/97
FORM IV SV-1 OLM03.0
353
4B EPA SAMPLE NO.
SEMIV9ILE METHOD BLANK SUMMARY •
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH069009A66
Instrument ID: 5972HP66
Matrix: (soil/water) SOIL
Level: (low/med) LOW
Contract: 68D50004
SAS No.:
SBLKAG
SDG No . : IlMPtiD
Lab Sample ID: 869009
Date Extracted: 09/19/97
Date Analyzed: 09/22/97
Time Analyzed: 0954
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD
COMMENTS:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
page 01 of 01
EPA
SAMPLE NO.
------------
DMP71
LAB
SAMPLE ID
--------------864715
••
LAB DATE
FILE ID ANALYZED ~ --------------=:;::;===::::===--
GR064715A66 09/22/97
FORM IV SV-1 OLM03.0
354
•
c. Method Blank: Summary (Form IV VOA)
' If 111ore than a single forn1 is necessary, forn1s shal I
. be arranged in chronological order by date of
analysis of the blarJ::: and by instru111ent.
. 25.
'
4A • EPA SAMPLE NO.
VOLATIL METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No.: 25633
Lab File ID: CB970822B55
Date Analyzed: 08/22/97
GC Colutn~ DB624
Instrument ID: F50055
ID: 0.53 (mm)
Contract: 68D50004
SAS No.:
VBLKTA
SDG No. : DMP63
Lab Sample ID: VBLKTA
Time Analyzed: 2054
Heated_Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
2_0
~ ;n
22
23
24
25
26
27
28
29
30
COMMENTS:
page 01 of 01
EPA
SAMPLE NO.
------------
DMP80
LAB
SAMPLE ID
--------------
864757
LAB TIME
FILE ID ANALYZED
------------------------
CN064757B55 2309
FORM IV VOA OLM03.0
26
• 4A • EPA SAMPLE NO.
VOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No.: 25633
Lab File ID: CB970824B55
Date Analyzed: 08/25/97
GC Colu~ ~ DB624
Instrument ID: F50055
ID: 0. 53 (mm)
Contract: 68D50004
SAS No.:
VBLKTJ
SDG No.: DMP63
Lab Sample ID: VBLKTJ
Time Analyzed: 0131
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
~ ,21
22
23
24
25
26
27
28
29
30
COMMENTS:
page 01 of 01
EPA
SAMPLE NO.
------------
VHBLKV5
LAB
SAMPLE ID
--------------
864756
LAB TIME
FILE ID ANALYZED
------------------------CN064756B55 0327
FORM IV VOA OLM03.0
27, -· . ; .
I 4A • EPA SAMPLE NO.
VOLATI METIJOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No.: 25633
Lab File ID: CB970822A55
Date Analyzed: 08/22/97
GC Col~~ DB624 ID: 0.53 (mm)
Instrument ID: F50055
Contract: 68D50004
SAS No.:
VBLKXG
SDG No.: DMP63
Lab Sample ID: VBLKXG
Time Analyzed: 0856
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO TIJE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20 _, Jl
22
23
24
25
26
27
28
29
30
COMMENTS:
page 01 of 01
EPA
SAMPLE NO.
------------
DMP63
DMP68
DMP69
LAB
SAMPLE ID
--------------
864749
864750
864751
LAB TIME
FILE ID ANALYZED
;::::;::::;::::;::::;::::;;::;::::_;;:;:::::::::::;::::;:::: ----------
CN064749A55 1525
CN064750A55 1603
CN064751A55 1644
FORM IV VOA OLM03.0
28
• 4A
VOLATI~ METHOD BLANK SUMMARY • EPA SAMPLE NO.
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: CB970823A55
Date Analyzed: 08/23/97
GC Col~·/: DB624 ID: 0. 53 (mm)
Instrument ID: F50055
Contract: 68D50004
SAS No.:
VBLKYY
SDG No.: DMP63
Lab Sample ID: VBLKYY
Time Analyzed: 0704
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
~ ~l
22
23
24
25
26
27
28
29
30
COMMENTS:
page 01 of 01
EPA
SAMPLE NO.
------------DMP79
DMP79MS
DMP79MSD
DMP98
LAB LAB TIME
SAMPLE ID FILE ID ANALYZED
--------------------------------------864752 CR064752A55 0752
864753 CR064753A55 1359
864 754 CR064754A55 1526
864758 CR064758A55 1605
FORM IV VOA OLM03.0
29
•
c. Method Blan!( Summary (Form IV VOA)
~, If n1ore than a single forn1 is necessary, forn1s shall
be arranged in chronological order by date of
analysis cif the blarJ::,; and by instru1nent.
42.
8 4A • EPA SAMPLE NO.
VOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No.: 25633
Lab File ID: GH064783A52
Date Analyzed: 08/19/97
GC Colu"it-i~ DB624
Instrument ID: F50052
ID: 0.53 (mm)
Contract: 68D50004
SAS No.:
VBLKV9
SDG No. : DLL03
Lab Sample ID: 864783
Time Analyzed: 1356
Heated Purge: (Y/N) Y
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
~o
"'.21
22
23
24
25
26
27
28
29
30
COMMENTS:
page 01 of 01
EPA
SAMPLE NO.
------------
DMH89
DMH90
DMH93
DMH96
DMH98
DMJ00
DMJ02
DMK07
DMK08
DMKl0
DMH89MS
DMH89MSD
LAB
SAMPLE ID
--------------
864678
864685
864686
864687
864688
864689
864690
864691
864692
864693
864679
864680
LAB TIME
FILE ID ANALYZED
------------------------
GH064678A52 1454
GH064685A52 1535
GH064686A52 1610
GH064687A52 1648
GH064688A52 1725
GH064689A52 1834
GH064690A52 1911
GH064691A52 1954
GH064692A52 2031
GH064693A52 2108
GH064679A52 2143
GH064680A52 2221
FORM IV VOA OLM03.0
43
• 4A • EPA SAMPLE NO.
VOLATILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No.: 25633
Lab File ID: GH064793A52
Date Analyzed: 08/20/97
GC Colu~~ DB624
Instrument ID: F50052
ID: 0.53 (mm)
Contract: 68D50004
SAS No.:
VBLKW5
SDG No.: DLL03
Lab Sample ID: 864793
Time Analyzed: 1304
Heated Purge: (Y/N) Y
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
~ 41
22
23
24
25
26
27
28
29
30
COMMENTS:
page 01 of 01
EPA
SAMPLE NO.
------------
DMK12
DMK14
DMP50
DMP53
DMP54
DMP55
LAB
SAMPLE ID
--------------
864694
864695
864696
864697
864698
864699
LAB TIME
FILE ID ANALYZED
------------------------GH064694B52 1537
GH064695B52 1623
GH064696B52 1702
GH064697B52 1742
GH064698B52 1818
GH064699B52 1858
FORM IV VOA OLM03.0
44
ft 4A
VOLATIN' METilOD BLANK SUMMARY • EPA SAMPLE NO.
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH064795B52
Date Analyzed: 08/21/97
GC Col~~ DB624 ID: 0.53 (mm)
Instrument ID: F50052
Contract: 68D50004
SAS No.:
VBLKW6
SDG No. : DLL03
Lab Sample ID: 864795
Time Analyzed: 1853
Heated Purge: (Y/N) Y
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
~ ;?1
22
23
24
25
26
27
28
29
30
COMMENTS:
page 01 of 01
EPA
SAMPLE NO.
-=--====----
DMP56
DMP58
DLL03
DLL04
VHBLKXl
LAB
SAMPLE ID
--------------
864700
864701
864 724
864725
864681
LAB TIME
FILE ID ANALYZED
=========== '== ----------GH064700B52 2036
GH064701B52 2120
GH064724B52 0201
GH064725B52 0249
GH064681B52 0326
FORM IV VOA OLM03.0
45
• •
. c. Method Blank Summary (Form IV SV)
J:If· more than a single form is necessary, forms shall be
arranged in chronological order by date of analysis and by
instrument.
353
'
ft 4B • EPA SAMPLE NO.
SEMivoMILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH069009A66
Instrument ID: 5972HP66
Matrix,J:(~oil/water) SOIL
Level: (low/med) LOW
Contract: 68D50004
SAS No.:
SBLKAG
SDG No. : DLL03
Lab Sample ID: 869009
Date Extracted: 09/19/97
Date Analyzed: 09/22/97
Time Analyzed: 0954
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
2-1
-· ~2
23
24
25
26
27
28
29
30
COMMENTS:
page 01 of 01
EPA
SAMPLE NO.
------------
DLL03
• LAB
SAMPLE ID
--------------
864724
. .
LAB DATE
FILE ID ANALYZED
----------,--------------
GR064724A66 09/22/97
. -
FORM IV SV-1 OLM03.0
354
A 4B • EPA SAMPLE NO.
SEMIVO~ILE METHOD BLANK SUMMARY
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GH064764A66
Instrument ID: 5972HP66
Matrix:..((~oil/water) SOIL
Level: (low/med) LOW
••
Contract: 68D50004
SAS No.:
SBLKRQ
SDG No. : DLL03
Lab Sample ID: 864764
Date Extracted: 08/15/97
Date Analyzed: 09/16/97
Time Analyzed: 1312
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
2-1
~ '2:2
COMMENTS:
23
24
25
26
27
28
29
30
---page 01 of 01
EPA
SAMPLE NO.
------------
DMJ-!89
DMH89MS
DMH89MSD
DMJ-!90
DMl-!93
DMJ-!96
DMJ02
DMK07
DMK08
DMKl0
DMK12
DMK14
DMP50
DMP53
DMP54
DMJ-!98
DMJ00
DMP55
DMP55DL
LAB
SAMPLE
---,-----
864678
864683
864684
864685
864686
864687
864690
864691
864692
864693,,
864694
864695
864696
864697
864698
864688
864689
864699
864699
LAB DATE
ID FILE ID ANALYZED
------------------------
GH064678A66 09/16/97
GH064683A66 09/16/97
GH064684A66 09/16/97
GH064685A66 09/16/97
GH064686A66 09/16/97
GH064687C66 09/17/97
GH064690C66 09/17/97
GH064691C66 09/17/97
GH064692C66 09/17/97
GH064693C66 09/17/97
GH064694C66 09/17/97
GH064695C66 09/17/97
GH064696C66 09/17/97
GH064697C66 09/17/97
GH064698C66 09/17/97
GH064688C66 09/17/97
GH064689C66 09/17/97
GH064699C66 09/17/97
GD064699A66 09/17/97
. -
FORM IV SV-1 OLM03.0
355
ft 4B
SEMIVOMILE METHOD BLANK SUMMARY • EPA SAMPLE NO.
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GJ064766A66
Instrument ID: 5972HP66
Matrix:~(~oil/water) SOIL
Level: (low/med) LOW
Contract: 68D50004
SAS No.:
SBLKRR
SDG No. : DLL03
Lab Sample ID: 864766
Date Extracted: 08/15/97
Date Analyzed: 09/18/97
Time Analyzed: 1117
THIS METHOD BLANK APPLIES TO THE FOLLOWING.SAMPLES, MS and MSD
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
2J.
.a ~2
23
24
25
26
27
28
29
30
COMMENTS:
EPA
SAMPLE NO.
------------
DMP58
DMP56
LAB
SAMPLE ID
===== .. ,. ::::::::=::::::;;;
864701
864700
.. '
LAB DATE
FILE ID ANALYZED
------------------------GJ064701A66 09/18/97
GJ064700A66 09/18/97
. -
FORM IV SV-1 OLM03.0
356
SEMIVO.ILE ~~OD BLANK SUMMARY •
EPA SAMPLE NO.
Lab Name: COMPUCHEM ENV. CORP.
Lab Code: COMPU Case No. : 25633
Lab File ID: GJ064768A66
Instrument ID: 5972HP66
Matrix~ (.iioil/water) SOIL
Level: (low/med) LOW ••
Contract: 68D50004
SAS No.:
SBLKRS
SDG No. : DLL03
Lab Sample ID: 864768
Date Extracted: 08/15/97
Date Analyzed: 09/17/97
Time Analyzed: 1428
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
2._l
-· £2
23
24
25
26
27
28
29
30
COMMENTS:
page 01 cit Lil
EPA
SAMPLE NO.
------------
DLL04
LAB
SAMPLE ID
--------------
864725
LAB DATE
FILE ID ANALYZED
============::;::;;:; ==========
GJ064725A66 09/19/97
. -
'flORM IV SV-1 OLM03.0
357
U.S. EPA -CLP •
SA
EPA SAMPLE NO.
SPIKE SAMPLE RECOVERY
MDLL03S
Lab Name: CHEMTECH CONSULTING GROUP
Lab Code: CHEM Case No. : 25633
Contract: 68-DS-0166
SAS No.: SDG No.: MDMP99
Matrix (soil/water) SOIL
i Solids for Sample: 36.8
Level (low/med): LOW
Concentration Units (ug/L or mg/kg dry weight) MG/KG
Control " •
' LiIBit Spiked Sample Sample Spike -
Analyte %R· Result (SSR) C Result (SR) C Added (SA) %R Q
---Aluminum
Antimony 75-125 204.0503 3.2133 B 198.35 101.3
Arsenic 75-125 21.0013 5.1214 15.87 100.1
Barium 75-125 1023.5401 228.9987 793.40 100.1
Beryllium 75-125 24.4684 2.6103 19.83 110.2
Cadmium 75-125 20.8347 0.3967 u 19.83 105.1
Calcium
Chromium 75-125 146.8264 62.9324 79.34 105.7
Cobalt 75-125 224.5636 22.1914 198.35 102.0
Copper 75-125 150.4998 41.5424 99.17 109.9
Iron
Lead 55.1690 46.4773 7.93 1.09. 6
Magnesium
Manganese 75-125 833.8345 627.3802 198.35 104.1
Mercury 75-125 1.2582 0.2717 u 1.36 92.5
Nickel 75-125 229.5977 27.4199 198.35 101.9
Potassium
Selenium 75-125 6.6050 2.8205 3.97 95.3
Silver 75-125 21.3662 0.7934 u 19.83 107.7
Sodium
Thallium 75-125 23.6790 3.0308 B 19.83 104.1
Vanadium 75-125 318.4148 105.0222 198.35 107.6
Zinc 75-125 347.0803 133.2037 198.35 107.8
Cyanide
---
Comments:
FORM V (Part 1) -IN 000036 ILM04.0
M
-NR
p
p
p
p
p
NR
p
p
p
NR
p
NR
p
CV
p
NR
p
p
NR
p
p
p
NR
-
U.S. EPA -CLP •
SA
EPA SAMPLE NO.
SPIKE SAMPLE RECOVERY
MDMK13S
Lab Name: CHEMTECH CONSULTING GROUP
Lab Code: CHEM Case No.: 25633
Contract: 68-DS-0166
SAS No.: SDG No. : MDMP98
Matrix (soil/water): WATER
% Solids for Sample: 0. 0
Level (low/med): LOW
Concentration Units (ug/L or mg/kg dry weight): UG/L
Control " • Limi:t Spiked Sample Sample Spike -
Analyte %R. Result (SSR) C Result (SR) C Added (SA) %R Q
---Aluminum 75-125 1991.7000 180.8400 B 2000.00 90.5
Antimony 75-125 483.5200 5.0000 u 500.00 96.7
Arsenic 75-125 44.9800 7.0000 u 40.00 112.4
Barium 75-125 1902.6900 24.2600 B 2000.00 93.9
Beryllium 75-125 53.3200 1.0000 u SO.DO 106.6
Cadmium 75-125 48.6800 1.0000 u SO.DO 97.4
Calcium
Chromium 75-125 198.2500 3.0400 B 200.00 97.6
Cobalt 75-125 485.2200 2.0000 u 500.00 97.0
Copper 75-125 243.6400 2.4200 B 250.00 96.5
Iron 75-125 2335.9400 1306.0000 1000.00 103 .. 0
Lead 75-125 18.7800 2.0000 u 20.00 93 .,9
Magnesium
Manganese 75-125 835.9600 347.1800 500.00 97.8
Mercury 75-125 0.8610 0.2000 u 1.00 86.1
Nickel 75-125 488.9900 2.8600 B SOD.DO 97.2
Potassium
Selenium 75-125 11.7600 5.0000 u 10.00 117.6
Silver 75-125 52.2600 2.0000 u 50.00 104.5
Sodium
Thallium 75-125 54.4400 6.0000 u 50.00 108.9
Vanadium 75-125 493.3800 1.0800 B SOD.OD 98.5
Zinc 75-125 497.7600 5.9200 B 500.00 98.4
Cyanide
---
Comments:
FORM V (Part 1) -IN 000047 ILM04.0
M
-p
p
p
p
p
p
NR
p
p
p
p
p
NR
p
CV
p
NR
p
p
NR
p
p
p
NR
-
• U.S. EPA -CLP
SA •
EPA SAMPLE NO.
SPIKE SAMPLE RECOVERY
MDMP63S
Lab Name: CHEMTECH CONSULTING GROUP
Lab Code: CHEM Case No. : 25633
Contract: 68-DS-0166
SAS No.: SDG No . : MDMP6 3
Matrix (soil/water): WATER Level (low/med): LOW
% Solids for .. sample: 0. 0
Concentration Units (ug/L or mg/kg dry weight): UG/L
Control " • Lim.i-t Spiked Sample Sample Spike -
Analyte %R. Result (SSR) C Result (SR) C Added (SA) %R Q
---Aluminum 75-125 1913.1300 55.5900 B 2000.00 92;9
Antimony 75-125 496.8200 5.0000 u 500.00 99.4
Arsenic 75-125 42.0200 7.0000 u 40.00 105.0
Barium 75-125 1957.8800 29.7200 B 2000.00 96.4
Beryllium 75-125 53.8100 1.0000 u 50.00 107.6
Cadmium 75-125 49.8900 1.0000 u 50.00 99.8
Calcium
Chromium 75-125 194.0200 1.0000 u 200.00 97.0
Cobalt 75-125 491.2200 2.0000 u 500.00 98.2
Copper 75-125 250.4200 1.0000 u 250.00 100.2
Iron 75-125 1272.4600 200.6100 1000.00 107.2
Lead 75-125 18.5000 2.0000 u 20.00 92.5
Magnesium
Manganese 75-125 537.5400 33.9700 500.00 100.7
Mercury 75-125 0.8660 0.2000 u 1.00 86.6
Nickel 75-125 495.9200 1.0000 u 500.00 99.2
Potassium
Selenium 75-125 12.0600 5.0000 u 10.00 120.6
Silver 75-125 53.0200 2.0000 u 50.00 106.0
Sodium
Thallium 75-125 51.4200 6.0000 u 50.00 102.8
Vanadium 75-125 504.7000 1.0000 u 500.00 100.9
Zinc 75-125 508.4200 2.0000 u 500.00 101.7
Cyanide
---
Comments:
FORM V (Part 1) -IN 000032 ILM04.0
M
-p
p
p
p
p
p
NR
p
p
p
p
p
NR
p
CV
p
NR
p
p
NR
p
p
p
NR
-
• U.S. EPA -CLP
SA •
EPA SAMPLE NO.
SPIKE SAMPLE RECOVERY
MDMP58S
Lab Name: CHEMTECH CONSULTING GROUP
Lab Code: CHEM Case No.: 25633
Contract: 68-DS-0166
SAS No.: SDG No. : MDMP58
Matrix (soil/water): SOIL
% Solids for Sample: 74.8
Level (low/med): LOW
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Control " • Limit Spiked Sample Sample Spike -
Analyte %R-Result (SSR) C Result (SR) C Added (SA) %R Q
---Aluminum
Antimony 75-125 118.6497 1.2855 u 128.55 92.3
Arsenic 75-125 12.2583 1.9796 B 10.28 100.0
Barium 75-125 549.2004 69.3130 514.19 93.3
Beryllium 75-125 13.2841 0.6170 B 12.85 98.6
Cadmium 75-125 11.8881 0.2571 u 12.85 92.5
Calcium
Chromium 75-125 66.0839 16.0711 51.42 97.3
Cobalt 75-125 127.9566 5.9466 B 128.55 94.9
Copper 75-125 71.7092 9.2452 64.27 97.2
Iron
Lead 56.2577 51.7585 5.14 87.5
Magnesium
Manganese 75-125 578.6508 460.0190 128.55 92.3
Mercury 75-125 0.7112 0.1337 u 0.67 106.1
Nickel 75-125 128.2960 6.7256 B 128.55 94.6
Potassium
Selenium 75-125 3.1880 1.2855 u 2.57 ·124.0
Silver 75-125 13.5181 0.5142 u 12.85 105.2
Sodium
Thallium 75-125 13.4513 1.5426 u 12.85 104.7
Vanadium 75-125 151.0721 24.0667 128.55 98.8
Zinc 75-125 169.7912 49.1670 128.55 93.8
Cyanide '
---
Comments:
FORM V (Part 1) -IN 000032 ILM04.0
M
-NR
p
p
p
p
p
NR
p
p
p
NR
p
NR
p
CV
p
NR
p
p
NR
p
p
p
NR
-
U.S. EPA -CLP •
6
EPA SAMPLE NO.
DUPLICATES
MDLL03D
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
SAS No.: Lab Code: CHEM Case No. : 25633
Matrix (soil/water) SOIL
% Solids for Sample: 36.8
SDG No.: MDMP99
Level (low/med): LOW
% Solids for Duplicate: 36.4
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Control
Analyte Limit Sample ( s) C Duplicate (D) C RPD,, • Q M -. ---- -Aluminum 55461.6630 56064.1860 1.1 p
Antimony 3.2133 B 2.6936 B 17.6 p
Arsenic 4.0 5.1214 3.6338 B 34.0 p
Barium 79.3 228.9987 230.6490 0.7 p
Beryllium 2.0 2.6103 2.6539 1.7 p
Cadmium 0.3967 u 0.3967 u p
Calcium 1698.4330 B 1731.7955 B 1.9 p
Chromium 62.9324 64.2098 2.0 ,p
Cobalt 19.8 22.1914 22.3699 0.8 p
Copper 9.9 41.5424 41.7645 0.5 p
Iron 44397.5484 45213.6584 1. 8 p
Lead 46.4773 47.7745 2.8 p
Magnesium 1983.5 4977.7253 5042.8951 1.3 p
Manganese 627.3802 637.6388 1.6 p
Mercury 0.2717 u 0.2717 u CV
Nickel 15.9 27.4199 27.9078 1.8 p
Potassium 1983.5 4203.7686 4229.8159 0.6 p
Selenium 2.0 2.8205 2.5746 9.1 p
Silver 0.7934 u 0.7934 u p
Sodium 300.2301 B 298.8416 B 0.5 p
Thallium 3.0308 B 3.4434 B 12.7 p
Vanadium 105.0222 106.6249 1. 5 p
Zinc 133.2037 136.3020 2.3 p
Cyanide NR
----
FORM VI -IN ILM04.0
000037
U.S. EPA -CLP •
6
EPA SAMPLE NO.
DUPLICATES
MDMK13D
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
SAS No.: Lab Code: CHEM Case No.: 25633 SDG No. : MDMP98
Matrix (soil/water) WATER Level (low/med): LOW
% Solids for Sample: 0.0 % Solids for Duplicate: 0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
Control
Analyte Limit Sample (S) C Duplicate (D) C RPD,.. • Q M -. -----Aluminum 180.8400 B 164.3800 B 9.5 p
Antimony 5.0000 u 5.0000 u p
Arsenic 7.0000 u 7.0000 u p
Barium 24.2600 B 24.4200 B 0.7 ,P
Beryllium 1.0000 u 1.0000 u p
Cadmium 1.0000 u 1.0000 u p
Calcium 5000.0 5981.2400 6053.1500 1.2 p
Chromium 3.0400 B 3.1400 B 3.2 p
Cobalt 2.0000 u 2.0000 u :P
Copper 2.4200 B 2.2200 B 8.6 p
Iron 1306.0000 1309.6200 0.3 p
Lead 2.0000 u 2.0000 u p
Magnesium 2408.7800 B 2418.7600 B 0.4 p
Manganese 347.1800 349.8300 0.8 p
Mercury 0.2000 u 0.2000 u CV
Nickel 2.8600 B 2.6800 B 6.5 p
Potassium 1437.8000 B 1428.4600 B 0.7 p
Selenium 5.0000 u 5.0000 u p
Silver 2.0000 u 2.0000 u p
Sodium 4503.7400 B 4535.7600 B 0.7 p
Thallium 6.0000 u 6.0000 u p
Vanadium 1.0800 B 1.0000 u 200.0 p
Zinc 5.9200 B 3.4500 B 52.7 p
Cyanide NR
----
FORM VI -IN 000048 ILM04.0
• U.S. EPA -CLP
6
DUPLICATES
•
EPA SAMPLE NO.
.... _ -
MDMP63D
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.: 25633 SAS No. : SDG No. : MDMP63
Matrix (soil/water) WATER Level (low/med): LOW
% Solids for Sample: 0.0 % Solids for Duplicate: 0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
Control
Analyte Limit Sample ( s) C Duplicate (D) C RPD,, • Q M -. ---- -Aluminum 55.5900 B 55.6000 B 0.0 p
Antimony 5.0000 u 5.0000 u p
Arsenic 7.0000 u 7.0000 u p
Barium 29.7200 B 29.8100 B 0.3 p
Beryllium 1.0000 u 1.0000 u p
Cadmium 1.0000 u 1.0000 u p
Calcium 4869.8400 B 4902.6000 B 0.7 p
Chromium 1.0000 u 1.0000 u p
Cobalt 2.0000 u 2.0000 u p
Copper 1.0000 u 1.0000 u p
Iron 100.0 200.6100 193.1600 3.8 p
Lead 2.0000 u 2.0000 u p
Magnesium 2343.4400 B 2355.2400 B 0.5 p
Manganese 15.0 33.9700 34.0200 0.1 p
Mercury 0.2000 u 0.2000 u CV
Nickel 1.0000 u 1.0000 u p
Potassium 1036.1100 B 1035.3800 B 0.1 p
Selenium 5.0000 u 5.0000 u p
Silver 2.0000 u 2.0000 u p
Sodium 2542.3000 B 2543". 0400 B 0.0 p
Thallium 6.0000 u 6.0000 u p
Vanadium 1.0000 u 1.0000 u p
Zinc 2.0000 u 2.0000 u p.
Cyanide NR
--- -
FORM VI -IN 000033 ILM04.0
U.S. EPA -CLP
6
DUPLICATES
•
EPA SAMPLE NO.
MDMP58D
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
SAS No.: Lab Code: CHEM Case No.: 25633
Matrix (soil/water): SOIL
% Solids for Sample: 74.8
SDG No. : MDMP58
Level (low/med): LOW
% Solids for Duplicat~: 74.3
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Control
Analyte Limit Sample ( s) C Duplicate (D) C RPD" ',; Q M -. ---- -Aluminum 7042.2151 7083.9212 0.6 p
Antimony 1.2855 u 1.2855 u p
Arsenic 1.9796 B 1.7997 u 200.0 ,p
Barium 51.4 69.3130 69.6447 0.5 p
Beryllium 0.6170 B 0.6222 B 0.8 p
Cadmium 0.2571 u 0.2571 u p
Calcium 455.6304 B 460.4741 B 1.1 p
Chromium 16.0711 16.2845 1. 3 p
Cobalt 5.9466 B 5.9466 B 0.0 p
Copper 6.4 9.2452 9.3609 1.2 p
Iron 12506.7462 12570.7014 0.5 p
Lead 51.7585 52.0953 0.6 p
Magnesium 1285.5 1983.4430 1994.0971 0.5 p
Manganese 460.0190 463.4461 0.7 p
Mercury 0.1337 u 0.1337 u CV
Nickel 6.7256 B 6.8285 B 1. 5 p
Potassium 1285.5 2037.7160 2045.4391 0.4 p
Selenium 1.2855 u 1.2855 u p
Silver 0.5142 u 0.5708 B 200.0 p
Sodium 106.6382 B 106.2526 B 0.4 p
Thallium 1.5426 u 1.5426 u p
Vanadium 12.9 24.0667 24.1901 0.5 p
Zinc 49.1670 49.4472 0.6 p
Cyanide NR
----
FORM VI -IN 000033 ILM04.0
• U.S. EPA -CLP •
7
LABORATORY CONTROL SAMPLE
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM
Solid LCS Source:
Aqueous LCS Source:
Case No.: 25633
EPA-LV
SAS No.:
Aqueous (ug/L) Solid
Analyte True Found %R True Found
Aluminum 308.7 282.1
Antimony -. 213.3 203.6 ' Arsenic 930.4 869.2
Barium 5.3 5.0
Beryllium 18.8 16.5
Cadmium 41.6 34.8
Calcium 184154.0 185245.2
Chromium 96.5 84.2
Cobalt 140.3 117.7
Copper 6680.2 5978.l
Iron 21012.1 19982.1
Lead 224.1 175.1
Magnesium 113189.0 99871.7
Manganese 201.2 175.2
Mercury 12.3 12.3
Nickel 56.8 46.6
Potassium 102.4 82.5
Selenium 37.0 34.8
Silver 20.9 19.8
Sodium 92.8 160.1
Thallium 38.1 33.9
Vanadium 65.8 55.8
Zinc 174.9 140.0
Cyanide
FORM VII -IN
SDG No.: MDMP99
(mg/kg)
C Limits %R
-193.1 ,;12;!.2 91.4
129.4 -297_2 95.5
613.4 1247.2 93.4
B 2.5 8.1 94.3
15.3 22.2 87.8
32.1 51.1 83.7
142933.0 225376.0 100.6
77.8 115.2 87.3
115.4 165.6 83.9
5727.3 7633.1 89.5
16831.3 25193.0 95.1
167.6 280.5 78.1
97493.0 128886.0 88.2
167.9 234.4 87.1
7.8 16.9 100.0
43.5 70.1 82.0
B 0.0 379.3 80.6
17.6 56.4 94.1
13.2 28.5 94.7
B 0.0 277.4 172.5
24.6 51.6 89.0
53.0 78.6 84.8
127.7 222.1 80.0
-
'! t
ILM04.0
000038
• U.S. EPA -CLP •
7
LABORATORY CONTROL SAMPLE --·-
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM
Solid LCS Source:
Case No.: 25633
Aqueous LCS Source: EPA-LV
Aqueous (ug/L)
Analyte True Found %R True
Aluminum 978.0 1060.32 108.4
Antimony 4&5·. 0 557.90 115.0
Arsenic 50-. 9 55.06 108.2
Barium 1004.5 1028.11 102.4
Beryllium 238.0 265.72 111.6
Cadmium 304.8 330.20 108.3
Calcium 25355.5 26844.78 105.9
Chromium 235.5 254.58 108.1
Cobalt 260.0 285.43 109.8
Copper 248.5 249.08 100.2
Iron 992.5 1126.62 113.5
Lead 2518.4 2745.73 109.0
Magnesium 12294.0 13479.52 109.6
Manganese 245.5 261.96 106.7
Mercury
Nickel 248.5 259.01 104.2
Potassium 24801.5 24312.66 98.0
Selenium 50.7 56.96 112.3
Silver 295.0 312.97 106.1
Sodium 24393.0 26640.14 109.2
Thallium 49.4 57.58 116.6
Vanadium 246.0 266.33 108.3
Zinc 1506.0 1698.34 112.8
Cyanide
SAS No.:
Solid
Found
FORM VII -IN
SDG No. : MDMP98
(mg/kg)
C Limits %R
-
" • -
-
000049
ILM04.0
• U.S. EPA -CLP •
7
LABORATORY CONTROL SAMPLE
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM
Solid LCS Source:
Case No.: 25633
Aqueous LCS Source: EPA-LV
Aqueous (ug/L)
Analyte True Found %R True
Aluminum 978.0 1053.36 107.7
Antimony 48-5·.o 557.38 114.9
Arsenic 50.9 55.52 109.1
Barium 1004.5 1023.80 101.9
Beryllium 238.0 263.96 110.9
Cadmium 304.8 327.78 107.5
Calcium 25355.5 26647.40 105.1
Chromium 235.5 253.48 107.6
Cobalt 260.0 283.67 109.1
Copper 248.5 247.90 99.8
Iron 992.5 1122.94 113.1
Lead 2518.4 2736.26 108.7
Magnesium 12294.0 13401.68 109.0
Manganese 245.5 260.80 106.2
Mercury
Nickel 248.5 257.20 103.5
Potassium 24801.5 24285.46 97.9
Selenium 50.7 55.18 108.8
Silver 295.0 311.75 105.7
Sodium 24393.0 26464.92 108.5
Thallium 49.4 57.44 116.3
Vanadium 246.0 265.08 107.8
Zinc 1506.0 1687.44 112.0
Cyanide
SAS No.:
Solid
Found
FORM VII -IN
SDG No. : MDMP63
(mg/kg)
C Limits %R
-,. .--
-
'! t
ILM04.0
U.S. EPA -CLP •
7
LABORATORY CONTROL SAMPLE
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM
Solid LCS Source:
Aqueous LCS Source:
Case No. : 25633
EPA-LV
SAS No.:
Aqueous (ug/L) Solid
Analyte True Found %R True Found
Aluminum 308.7 321.3
Antimony -. 213.3 205.1 Arsenic 930.4 929.1 Barium 5.3 5.7 Beryllium 18.8 17.7
Cadmium 41.6 38.1 Calcium 184154.0 170858.6
Chromium 96.5 91.2
Cobalt 140.3 128.5
Copper 6680.2 6096.2
Iron 21012.1 21255.2
Lead 224.1 195.6
Magnesium 113189.0 102344.5
Manganese 201.2 187.6
Mercury 12.3 12.2
Nickel 56.8 51.1
Potassium 102.4 101.0
Selenium 37.0 38.8
Silver 20.9 21. 0 Sodium 92.8 197.2
Thallium 38.1 33.3 Vanadium 65.8 59.5
Zinc 174.9 158.2
Cyanide
FORM VII -IN
SDG No. : MDMP58
(mg/kg)
C Limits %R
-193.1 "4 :¥4 . 2 104.1 -129.4 297 .,2 96.2
613.4 1247.2 99.9
B 2.5 8.1 107.5
15.3 22.2 94.1
32.1 51.1 91.6
142933.0 225376.0 92.8
77.8 115.2 94.5
115.4 165.6 91.6
5727.3 7633.1 91. 3
16831.3 25193.0 101.2
167.6 280.5 87.3
97493.0 128886.0 90.4
167.9 234.4 93.2
7.8 16.9 99.2
43.5 70.1 90.0
B 0.0 379.3 98.6
17.6 56.4 104.9
13.2 28.5 100.5
B 0.0 277. 4 212.5
24.6 51. 6 87.4
53.0 78.6 90.4
127.7 222.1 90.5
-
000034 ILM04.0
..
MEMORANDUM
Date: 12/11/97
• •
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of METALS INORGANIC Sample Analysis RECE/\lf::O
DE:c 19 1997
SUPERFUND SECTION
97-0329 JOHNSON CONTRO~S·GLOBE
WINSTON-SALEM, NC
From: Keith Bates ~~
To: PAT DEROSA
Thru: QA Office
Please substitute the lead results for those reported September 16, 1997. The original laboratory, Antee Ltd.,
reanalyzed lead by graphite furnace due to suspected ICP interference. All other metal results remain the same
as those previously reported.
The Region IV, Science and Ecosystem Support Division reanalyzed the samples for all metals. Those results,
reported on November 26, 1997, should be used for decision purposes.
If you have any questions, please contact me.
ATTACHMENT
•
INORGANIC DATA REVIEW DOCUMENT
United States Environmental Protection Agency
Region IV
Environmental Services Division
980 College Station Road, Athens, GA 30613
Date: 11 December 1997
Subject: Review of. Inorganic Contract Data
Case No. 25633 SAS No.
Contract Lab Name:~An=t~e~c=h~L=t=d=·-----------
Region Iv: Project No.: 97-0329
SMO Traffic Nos.: MDMP65. MDMP70-MDMP78
Reg. IV SAD Nos. :~1=2~1~1~6~-~1=2=4~7~5 ___________ _
Matrix types: Water __ Soil/Sed . ..J.Q_ Waste
Review performed by:_.,K~e~iut"h.._,B~a~t~e,._..s ______________ _
Review Codes
A-Acceptable: All QC criteria met. No data qualified based on these
items.
P-Provisional: Some QC criteria were exceeded resulting in data
qualifiers being assigned based on these items.
u-unacceptable: The QC criteria were exceeded to such an extent that
the associated data was rejected based on these items.
N/A-Not Applicable: This item does not apply to the case being
reviewed.
I. Sample Holding Times (Technical holding times; waters only)
Metals (6 mos.)
Mercury (28 days)
Cyanide (14 days)
NIA
NIA
NIA
Remarks: Soil samples only.
II. Calibration
Initial Calib.
Init. Cal. Ver.
Cont. Cal. Ver.
ICP Furnace
A
A
A
•
Mercury CN
Remarks: CRA ran at 2X CRDL instead of at the CRDL as required by
the functional guidelines, but all sample results are greater than
2X CRDL. The CCV was ran at the same concentration as the ICV.
III. Blanks
Calibration Blanks
Preparation Blanks
Blind Blanks
Remarks:
A
A
NIA
IV. ICP Interference Check Sample
False Positives
False Negatives
Remarks:
NIA
NIA
V. Spiked Sample Results
Matrix Spike
Blind Spike
Water
NIA
NIA
Soil
A
NIA
Remarks: The lead matrix spike recovery was 3828%. The data is
not flagged because the sample concentration is greater than 4X
the spike concentration.
VI. Other QC
Matrix Duplicates A
LCS A
Serial Dilution Results NIA
Linear Range Check (2xCRDL) NIA
Remarks:
VII. Deliverables
Cover Page NIA
Form I A
QC Summary Forms A
Raw Data
Traffic Reports
Digestion Logs
Preparation Logs
Run Logs
A
N/A
N/A
A
A
•
Remarks: Sample prepared for ICP analysis were used to run the
graphite furnace analysis.
VIII. Contact with Contract Lab required during data review?
Yes No_x__
Remarks:
METALS SAMPLE ANALYSIS
Sample 12476 FY 1997
METALS SCAN
Project: 97-0329
EPA-REGION IV SESD, ATHENS, GA
THIS TEST SET IS INCOMPLETE
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB010SL MD Number: MP65
Media: SOIL
RESULTS UNITS
13000J MG/KG
0.6UJ MG/KG
0.96J MG/KG
100J · MG/KG
0.85J MG/KG
4.1JN MG/KG
1100J MG/KG
32J MG/KG
18J MG/KG
20J MG/KG
19000J MG/KG
34 MG/KG
2500J MG/KG
760J MG/KG
0.34J MG/KG
19J MG/KG
2200J MG/KG
0.32U MG/KG
2.6J MG/KG
54 MG/KG
0.36UJ MG/KG
51J MG/KG
370J MG/KG
23 %
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/9717:20
Ending:
Production Date: 12/11/97 09:48
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
METALS SAMPLE ANALYSIS
Sample 12477 FY 1997
METALS SCAN
EPA-REGION IV SESD, ATHENS, GA
Project: 97-0329
THIS TEST SET IS INCOMPLETE
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
ld/Station:JB001SL MD Number: MP70 lnorg Contractor: ANTEC
Media: SOIL
RESULTS UNITS ANALYTE
6200J MG/KG ALUMINUM
0.58UJ MG/KG ANTIMONY
1UJ MG/KG ARSENIC
53J MG/KG BARIUM
0.57J MG/KG BERYLLIUM
2.3J MG/KG CADMIUM
490J MG/KG CALCIUM
20J MG/KG CHROMIUM
9.BJ MG/KG COBALT
14J MG/KG COPPER
8700J MG/KG IRON
17 MG/KG LEAD
1600J MG/KG MAGNESIUM
210J MG/KG MANGANESE
0.0BUJ MG/KG TOTAL MERCURY
10J MG/KG NICKEL
1000J MG/KG POTASSIUM
0.31U MG/KG SELENIUM
2.3J MG/KG SILVER
46 MG/KG SODIUM
0.36U MG/KG THALLIUM
25J MG/KG VANADIUM
32J MG/KG ZINC
14 % % MOISTURE
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/9717:15
Ending:
Production Date: 12/11/97 09:48
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12478 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97--0329
THIS TEST SET IS INCOMPLETE
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
ld/Station:JB101SL MD Number: MP71 lnorg Contractor: ANTEC
Media: SOIL
RESULTS UNITS ANALYTE
6000J MG/KG ALUMINUM
0.64UJ MG/KG ANTIMONY
0.84J MG/KG ARSENIC
65J MG/KG BARIUM
0.61J MG/KG BERYLLIUM
2.2J MG/KG CADMIUM
640J MG/KG CALCIUM
19J MG/KG CHROMIUM
10J MG/KG COBALT
15J MG/KG COPPER
8400J MG/KG IRON
19 MG/KG LEAD
1600J MG/KG MAGNESIUM
370J MG/KG MANGANESE
0.12UJ MG/KG TOTAL MERCURY
9.7J MG/KG NICKEL
1000J MG/KG POTASSIUM
0.34U MG/KG SELENIUM
2.1J MG/KG SILVER
38 MG/KG SODIUM
0.39U MG/KG THALLIUM
25J MG/KG VANADIUM
30J MG/KG ZINC
15 % %MOISTURE
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/9717:15
Ending:
Production Date: 12/11/97 09:48
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and rean?lysis is necessary for verification.
C-confirmed by gems: 1.when no value ls reported, see chlordane constituents 2.constituents or metabolites of te~hnical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12479 FY 1997
METALS SCAN
Project: 97-0329
EPA -REGION IV SESD, ATHENS, GA
THIS TEST SET IS INCOMPLETE
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
ld/Station:JB003SL MD Number: MP72 lnorg Contractor: ANTEC
Media: SOIL
RES UL TS UNITS
7500J MG/KG
0.59UJ MG/KG
0.49UR MG/KG
53J MG/KG
0.69JN MG/KG
3.4JN MG/KG
1600J MG/KG
26J MG/KG
10J MG/KG
21J MG/KG
16000J MG/KG
7.6 MG/KG
4200J MG/KG
370J MG/KG
0.09UJ MG/KG
16J MG/KG
1800J MG/KG
0.32U MG/KG
2.7J MG/KG
370 MG/KG
0.36UJ MG/KG
47J MG/KG
52J MG/KG
14 %
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 18:30
Ending:
Production Date: 12/11/97 09:48
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no Value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12480 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0329
THIS TEST SET IS INCOMPLETE
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
Id/Station: JB004SL MD Number: MP73 lnorg Contractor: ANTEC
Media: SOIL
RESULTS UNITS ANALYTE
13000J MG/KG ALUMINUM
0.51UJ MG/KG ANTIMONY
1.3J MG/KG ARSENIC
83J MG/KG BARIUM
0.99J MG/KG BERYLLIUM
4.1JN MG/KG CADMIUM
1200J MG/KG CALCIUM
27J MG/KG CHROMIUM
13J MG/KG COBALT
29J MG/KG COPPER
20000J MG/KG IRON
72 MG/KG LEAD
3100J MG/KG MAGNESIUM
650J MG/KG MANGANESE
0.11 UJ MG/KG TOTAL MERCURY
19J MG/KG NICKEL
2100J MG/KG POTASSIUM
0.27U MG/KG SELENIUM
2.6J MG/KG SILVER
97 MG/KG SODIUM
0.31UJ MG/KG THALLIUM
53J MG/KG VANADIUM
100J MG/KG ZINC
7 % % MOISTURE
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:45
Ending:
Production Date: 12/11/97 09:48
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R--qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12481 FY 1997 Project: 97-0329
METALS SCAN THIS TEST SET IS INCOMPLETE
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
ld/Station:JB005SL MD Number: MP74 lnorg Contractor: ANTEC
Media: SOIL
RESULTS UNITS ANALYTE
14000J MG/KG ALUMINUM
0.52UJ MG/KG ANTIMONY
1.5J MG/KG ARSENIC
76J MG/KG BARIUM
0.64JN MG/KG BERYLLIUM
4.2JN MG/KG CADMIUM
4500J MG/KG CALCIUM
28J MG/KG CHROMIUM
8.8J MG/KG COBALT
27J MG/KG COPPER
20000J MG/KG IRON
18 MG/KG LEAD
3300J MG/KG MAGNESIUM
270J MG/KG MANGANESE
0.11 UJ MG/KG TOTAL MERCURY
14J MG/KG NICKEL
2900J MG/KG POTASSIUM
0.28U MG/KG SELENIUM
2.4J MG/KG SILVER
98 MG/KG SODIUM
0.32UJ MG/KG THALLIUM
52J MG/KG VANADIUM
54J MG/KG ZINC
12 % %MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:00
Ending:
Production Date: 12/11/97 09:48
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12482 FY 1997 Project: 97-0329
METALS SCAN THIS TEST SET IS INCOMPLETE
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
ld/Station:JB006SL MD Number: MP75 lnorg Contractor: ANTEC
Media: SOIL
RESULTS UNITS ANALYTE
15000J MG/KG ALUMINUM
0.78UJ MG/KG ANTIMONY
2.2J MG/KG ARSENIC
82J MG/KG BARIUM
0.95JN MG/KG BERYLLIUM
5.3JN MG/KG CADMIUM
4700J MG/KG CALCIUM
36J MG/KG CHROMIUM
14J MG/KG COBALT
62J MG/KG COPPER
26000J MG/KG IRON
2300 MG/KG LEAD
3500J MG/KG MAGNESIUM
510J MG/KG MANGANESE
0.15UJ MG/KG TOTAL MERCURY
23J MG/KG NICKEL
2300J MG/KG POTASSIUM
0.42U MG/KG SELENIUM
3.5J MG/KG SILVER
820 MG/KG SODIUM
0.47UJ MG/KG THALLIUM
68J MG/KG VANADIUM
180J MG/KG ZINC
38 % %MOISTURE
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/9719:00
Ending:
Production Date: 12/11/97 09:48
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12483 FY 1997
METALS SCAN
Project: 97-0329
EPA -REGION IV SESD, ATHENS, GA
THIS TEST SET IS INCOMPLETE
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JB007SL MD Number: MP76
Media: SOIL
RESULTS UNITS
17000J MG/KG
0.61 UJ MG/KG
1.9J MG/KG
88J MG/KG
0.83JN MG/KG
5.2JN MG/KG
1200J MG/KG
43J MG/KG
13J MG/KG
27J MG/KG
24000J MG/KG
1100 MG/KG
3200J MG/KG
650J MG/KG
0.13UJ MG/KG
25J MG/KG
3100J MG/KG
0.33U MG/KG
2.9J MG/KG
70 MG/KG
0.38UJ MG/KG
54J MG/KG
110J MG/KG
21 %
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:30
Ending:
Production Date: 12/11/97 09:48
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12484 FY 1997
METALS SCAN
Project: 97-0329
EPA-REGION IV SESD, ATHENS, GA
THIS TEST SET IS INCOMPLETE
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JB008SL MD Number: MP77
Media: SOIL
RESULTS UNITS
13000J MG/KG
0.64UJ MG/KG
0.53UR MG/KG
130J MG/KG
1JN MG/KG
4.5JN MG/KG
710J MG/KG
27J MG/KG
14J MG/KG
27J MG/KG
21000J MG/KG
70 MG/KG
4100J MG/KG
1000J MG/KG
0.14UJ MG/KG
23J MG/KG
4800J MG/KG
0.34U MG/KG
4.2J MG/KG
76 MG/KG
0.39UJ MG/KG
45J MG/KG
77J MG/KG
28 %
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:35
Ending:
Production Date: 12/11/97 09:48
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12485 FY 1997
METALS SCAN
Project: 97-0329
EPA -REGION IV SESD, ATHENS, GA
THIS TEST SET IS INCOMPLETE
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
Id/Station: JB009SL MD Number: MP78 lnorg Contractor: ANTEC
Media: SOIL
RESULTS UNITS
7500J MG/KG
1UJ MG/KG
1UJ MG/KG
87J MG/KG
0.54J MG/KG
2.7JN MG/KG
960J MG/KG
16J MG/KG
9.6J MG/KG
20J MG/KG
12000J MG/KG
70 MG/KG
2600J MG/KG
710J MG/KG
0.07UJ MG/KG
15J MG/KG
2800J MG/KG
0.31U MG/KG
1.7J MG/KG
58 MG/KG
0.35U MG/KG
26J MG/KG
71J MG/KG
8 %
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 21:45
Ending:
Production Date: 12/11/97 09:48
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
I '
•
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
MEMORANDUM
Date: 11/26/97
Subject: Results of METALS INORGANIC Sample Analysis
98-0053 Johnsons Controls Globe
Winston Salem, NC
From: Terri White ~ ~
To: Jennifer Wendel
WMD
CC: Pat DeRosa
NC
Thru: Jenny Scifres -l ;?.~,e:,
Chief, INORGANIC Chemistry Section
RECEIVED
DEC O 8 1997
SUPERFUND ~Elil"ION
Attached are the results of analysis of samples collected as part of the subject project. If you have any
questions, please contact me.
ATTACHMENT
METALS SAMPLE ANALYSIS
Sample 466 FY 1998 Project: 98-0053
METALS SCAN
Facility: Johnsons Controls Globe
Program: SSF
Id/Station: MDMP65
Media: SOIL
RESULTS UNITS ANALYTE
3.0U MG/KG SILVER
6.8 MG/KG ARSENIC
NA MG/KG BORON
100 MG/KG BARIUM
1.5U MG/KG BERYLLIUM .
1.5U MG/KG CADMIUM
16 MG/KG COBALT
48 MG/KG CHROMIUM
24 MG/KG COPPER
3.0U MG/KG MOLYBDENUM
14 MG/KG NICKEL.
32 MG/KG LEAD
12U MG/KG ANTIMONY
12U MG/KG SELENIUM
7.5U MG/KG TIN
4.0 MG/KG STRONTIUM
15U MG/KG TELLURIUM
1300 MG/KG TITANIUM
30U MG/KG THALLIUM
78 MG/KG VANADIUM
17 MG/KG YTTRIUM
430 MG/KG ZINC
NA MG/KG ZIRCONIUM
Winston Salem, NC
0.05U MG/KG TOTAL MERCURY
31000 MG/KG ALUMINUM
720 MG/KG MANGANESE
1100 MG/KG CALCIUM
2700 MG/KG MAGNESIUM
35000 MG/KG IRON
300U MG/KG SODIUM
2800 MG/KG POTASSIUM
22 % % MOISTURE
EPA-REGION IV SESD, ATHENS, GA
Produced by: Terri White
Requestor: Jennifer Wendel
Project Leader:
Beginning: 10/29/97 15:35
Ending:
Production Date: 11/26/97 15:31
REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. l-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indic:-ites that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
METALS SAMPLE ANALYSIS
Sample 467 FY 1998 Project: 98--0053
METALS SCAN
Facility: Johnsons Controls Globe
Program: SSF
Id/Station: MDMP70
Media: SOIL
RESULTS UNITS ANALYTE
2.0U MG/KG SILVER
2.6 MG/KG ARSENIC
NA MG/KG BORON
88 MG/KG BARIUM
1.0U MG/KG BERYLLIUM
1.0U MG/KG CADMIUM . 12 MG/KG COBALT
36 MG/KG CHROMIUM
21 MG/KG COPPER
2.0U MG/KG MOLYBDENUM
9.2 MG/KG NICKEL
27 MG/KG LEAD
8.0U MG/KG ANTIMONY
8.0U MG/KG SELENIUM
5.0U MG/KG TIN
5.6 MG/KG STRONTIUM
10U MG/KG TELLURIUM
1100 MG/KG TITANIUM
20U MG/KG THALLIUM
48 MG/KG VANADIUM
10 MG/KG YTTRIUM
33 MG/KG ZINC
NA MG/KG ZIRCONIUM
Winston Salem, NC
0.05U MG/KG TOTAL MERCURY
17000 MG/KG ALUMINUM
320 MG/KG MANGANESE
. 440 MG/KG CALCIUM
2400 MG/KG MAGNESIUM
20000 MG/KG IRON
200U MG/KG SODIUM
1800 MG/KG POTASSIUM
11 % % MOISTURE
EPA -REGION IV SESD, ATHENS, GA
Produced by: Terri White
Requester: Jennifer Wendel
Project Leader:
Beginning: 10/29/97 15:35
Ending:
Production Date: 11/26/97 15:31
REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actuat value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indic&!es that data unusable. compound may or may not be present. resampfing and reanalysis Is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
e
•
METALS SAMPLE ANALYSIS
Sample 468 FY 1998 Project: 98--0053
METALS SCAN
Facility: Johnsons Controls Globe
Program: SSF
Id/Station: MOMP71
Media: SOIL
RESULTS UNITS ANALYTE
2.0U MG/KG SILVER.
2.5 MG/KG ARSENIC
NA MG/KG BORON
88 MG/KG BARIUM
1.0U MG/KG BERYLLIUM
1.0U MG/KG CADMIUM
13 MG/KG COBALT
35 MG/KG CHROMIUM
21 MG/KG COPPER
2.0U MG/KG MOLYBDENUM
9.3 MG/KG NICKEL
25 MG/KG LEAD
8.0U MG/KG ANTIMONY
8.0U MG/KG SELENIUM
6.5U MG/KG TIN
54 MG/KG STRONTIUM
10U MG/KG TELLURIUM
1200 MG/KG TITANIUM
20U MG/KG THALLIUM
48 MG/KG VANADIUM
11 MG/KG YTTRIUM
33 MG/KG ZINC
NA MG/KG ZIRCONIUM
Winston Salem, NC
0.05U MG/KG TOTAL MERCURY
16000 MG/KG ALUMINUM
340 MG/KG MANGANESE
420 MG/KG CALCIUM
2400 MG/KG MAGNESIUM
20000 MG/KG IRON
200U MG/KG SODIUM
1800 MG/KG POTASSIUM
11 % % MOISTURE
EPA -REGION IV SES0, ATHENS, GA
-A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Terri White.
Requester: Jennifer Wendel
Project Leader:
Beginning: 10/29/97 15:35
Ending:
Production Date: 11/26/97 15:31
REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value ls reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
METALS SAMPLE ANALYSIS
Sample 469 FY 1998 Project: 98-0053
METALS SCAN
Facility: Johnsons Controls Globe
Program: SSF
Id/Station: MDMP72
Media: SOIL
RESULTS UNITS ANALYTE
3.0U MG/KG SILVER
2.1 MG/KG ARSENIC
NA MG/KG BORON
90 MG/KG BARIUM
1.SU MG/KG BERYLLIUM
1.5U MG/KG CADMIUM
12 MG/KG COBALT
34 MG/KG CHROMIUM
32 MG/KG COPPER
3.0U MG/KG MOLYBDENUM
16 MG/KG NICKEL
13 MG/KG LEAD
12U MG/KG ANTIMONY
15U MG/KG SELENIUM
7.8U MG/KG TIN
16 MG/KG STRONTIUM
15U MG/KG TELLURIUM
1900 MG/KG TITANIUM
30U MG/KG THALLIUM
78 MG/KG VANADIUM
12 MG/KG YTTRIUM
61 MG/KG ZINC
NA MG/KG ZIRCONIUM
Winston Salem, NC
o.osu MG/KG TOTAL MERCURY
22000 MG/KG ALUMINUM
710 MG/KG MANGANESE
3000 MG/KG CALCIUM
6600 MG/KG MAGNESIUM
31000 MG/KG IRON
600 MG/KG SODIUM
3300 MG/KG POTASSIUM
12 % % MOISTURE
EPA -REGION IV SESD, ATHENS, GA
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Terri White
Requester: Jennifer Wendel
Project Leader:
Beginning: 10129197 15:35
Ending:
Production Date: 11/26/97 15:31
REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampting and reanalysis is necessary for verification.
C-confirmed by gems: t .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
e
•
METALS SAMPLE ANALYSIS
Sample 470 FY 1998 Proiect: 98--0053
METALS SCAN
Facility: Johnsons Controls Globe
Program: SSF
Id/Station: MDMP73
Media: SOIL
RESULTS UNITS ANALYTE
3.0U MG/KG SILVER
4.3 MG/KG ARSENIC
NA MG/KG BORON
130 MG/KG BARIUM
1.5U MG/KG BERYLLIUM
1.5U MG/KG CADMIUM
15 MG/KG COBALT
41 MG/KG CHROMIUM
44 MG/KG COPPER
4.2 MG/KG MOLYBDENUM
19 MG/KG NICKEL
130 MG/KG LEAD
12U MG/KG ANTIMONY
15U MG/KG SELENIUM
7.5U MG/KG TIN
11 MG/KG STRONTIUM
15U MG/KG TELLURIUM
1600 MG/KG TITANIUM
30U MG/KG THALLIUM
85 MG/KG VANADIUM
23 MG/KG YTTRIUM
140 MG/KG ZINC
NA MG/KG ZIRCONIUM
Winston Salem, NC
0.05U MG/KG TOTAL MERCURY
34000 MG/KG ALUMINUM
1100 MG/KG MANGANESE
2100 MG/KG CALCIUM
4900 MG/KG MAGNESIUM
36000 MG/KG IRON
300U MG/KG SODIUM
3400 MG/KG POTASSIUM
35 % % MOISTURE
EPA -REGION IV SESD, ATHENS, GA
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Terri White
Requester: Jennifer Wendel
Project Leader:
Beginning: 10129197 15:35
Ending:
Production Date: 11/26/97 15:31
REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 471 FY 1998 Project: 98-0053
METALS SCAN
Facility: Johnsons Controls Globe
Program: SSF
ld/Station:MDM P74
Media: SOIL
RESULTS UNITS ANALYTE
4.0U MG/KG SILVER
5.2 MG/KG ARSENIC
NA MG/KG BORON
120 MG/KG BARIUM
2.0U MG/KG BERYLLIUM
2.0U MG/KG CADMIUM
8.6 MG/KG COBALT
38 MG/KG CHROMIUM
40 MG/KG COPPER
8.2 MG/KG MOLYBDENUM
15 MG/KG NICKEL
23 MG/KG LEAD
16U MG/KG ANTIMONY
16U MG/KG SELENIUM
10U MG/KG TIN
26 MG/KG STRONTIUM
20U MG/KG TELLURIUM
1400 MG/KG TITANIUM
40U MG/KG THALLIUM
77 MG/KG VANADIUM
8.6 MG/KG YTTRIUM
68 MG/KG ZINC
NA MG/KG ZIRCONIUM
Winston Salem, NC
0.05U MG/KG TOTAL MERCURY
37000 MG/KG ALUMINUM
390 MG/KG MANGANESE
5800 MG/KG CALCIUM
5100 MG/KG MAGNESIUM
32000 MG/KG IRON
400U MG/KG SODIUM
5100 MG/KG POTASSIUM
10 % % MOISTURE
EPA -REGION IV SESD, ATHENS, GA
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Terri White
Requester: Jennifer Wendel
Project Leader:
Beginning: 10/29/97 15:35
Ending:
Production Date: 11/26/97 15:31
REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
K-actual Value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
METALS SAMPLE ANALYSIS
Sample 472 FY 1998 Project: 98-0053
METALS SCAN
Facility: Johnsons Controls Globe
Program: SSF
Id/Station: MDMP75
Media: SOIL
RESULTS UNITS ANALYTE
4.0U MG/KG SILVER
9.4 MG/KG ARSENIC
NA MG/KG BORON
130 MG/KG BARIUM
2.0U MG/KG BERYLLIUM
2.0U MG/KG CADMIUM
14 MG/KG COBALT
48 MG/KG CHROMIUM
45 MG/KG COPPER
4.0U MG/KG MOLYBDENUM
21 MG/KG NICKEL
3300 MG/KG LEAD
16U MG/KG ANTIMONY
25U MG/KG SELENIUM
10U MG/KG TIN
21 MG/KG STRONTIUM
20U MG/KG TELLURIUM
1400 MG/KG TITANIUM
40U MG/KG THALLIUM
110 MG/KG VANADIUM
17 MG/KG YTTRIUM
300 MG/KG ZINC
NA MG/KG ZIRCONIUM
Winston Salem, NC
0.07 MG/KG TOTAL MERCURY
45000 MG/KG ALUMINUM
860 MG/KG MANGANESE
9000 MG/KG CALCIUM
4100 MG/KG MAGNESIUM
50000 MG/KG IRON
1200 MG/KG SODIUM
3300 MG/KG POTASSIUM
36 % % MOISTURE
EPA -REGION IV SESD, ATHENS, GA
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Terri White
Requester: Jennifer Wendel
Project Leader:
Beginning: 10/29/97 15:35
Ending:
Production Date: 11/26/97 15:31
REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
e
•
METALS SAMPLE ANALYSIS
Sample 473 FY 1998 Project: 98--0053
METALS SCAN
Facility: Johnsons Controls Globe
Program: SSF
Id/Station: MDMP76
Media: SOIL
RESULTS UNITS ANALYTE
4.0U MG/KG SILVER
7.2 MG/KG ARSENIC
NA MG/KG BORON
150 MG/KG BARIUM
2.0U MG/KG BERYLLIUM
2.0U MG/KG CADMIUM
16 MG/KG COBALT
40 MG/KG CHROMIUM
40 MG/KG COPPER
4.0U MG/KG MOLYBDENUM
20 MG/KG NICKEL
1800 MG/KG LEAD
16U MG/KG ANTIMONY
16U MG/KG SELENIUM
10U MG/KG TIN
15 MG/KG STRONTIUM
20U MG/KG TELLURIUM
2100 MG/KG TITANIUM
40U MG/KG THALLIUM
86 MG/KG VANADIUM
18 MG/KG YTTRIUM
160 MG/KG ZINC
NA MG/KG ZIRCONIUM
Winston Salem, NC
0.05U MG/KG TOTAL MERCURY
47000 MG/KG ALUMINUM
1200 MG/KG MANGANESE
2200 MG/KG CALCIUM
5000 MG/KG MAGNESIUM
43000 MG/KG IRON
400U MG/KG SODIUM
5500 MG/KG POTASSIUM
18 % % MOISTURE
EPA -REGION IV SESD, ATHENS, GA
A-average value. NA-nOt analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Terri White
Requester: Jennifer Wendel
Project Leader:
Beginning: 10/29/97 15:35
Ending:
Production Date: 11/26/97 15:31
REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
e
•
METALS SAMPLE ANALYSIS
Sample 474 FY 1998 Project: 98-0053
METALS SCAN
Facility: Johnsons Controls Globe
Program: SSF
Id/Station: MDMP77
Media: SOIL
RESULTS UNITS ANALYTE
3.0U MG/KG SILVER
4.1 MG/KG ARSENIC
NA MG/KG BORON
180 MG/KG BARIUM
1.5U MG/KG BERYLLIUM
1.5U MG/KG CADMIUM
13 MG/KG COBALT
25 MG/KG CHROMIUM
29 MG/KG COPPER
3.0U MG/KG MOLYBDENUM
14 MG/KG NICKEL
94 MG/KG LEAD
12U MG/KG ANTIMONY
12U MG/KG SELENIUM
15U MG/KG TIN
6.1 MG/KG STRONTIUM
15U MG/KG TELLURIUM
2400 MG/KG TITANIUM
30U MG/KG THALLIUM
57 MG/KG VANADIUM
22 MG/KG YTTRIUM
88 MG/KG ZINC
NA MG/KG ZIRCONIUM
Winston Salem, NC
0.05U MG/KG TOTAL MERCURY
30000 MG/KG ALUMINUM
1500 MG/KG MANGANESE
850 MG/KG CALCIUM
5400 MG/KG MAGNESIUM
32000 MG/KG IRON
300U MG/KG SODIUM
6900 MG/KG POTASSIUM
7 % % MOISTURE
EPA-REGION IV SESD, ATHENS, GA
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Terri White
Requestor: Jennifer Wendel
Project Leader:
Beginning: 10/29/97 15:35
Ending:
Production Date: 11/26/97 15:31
REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no vatue is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
METALS SAMPLE ANALYSIS
Sample 475 FY 1998 Project: 98-0053
METALS SCAN
Facility: Johnsons Controls Globe
Program: SSF
Id/Station: MDMP78
Media: SOIL
RESULTS UNITS ANALYTE
3.0U MG/KG SILVER
1.8 MG/KG ARSENIC
NA MG/KG BORON
130 MG/KG BARIUM
1.5U MG/KG BERYLLIUM
1.5U MG/KG CADMIUM
11 MG/KG COBALT
22 MG/KG CHROMIUM
23 MG/KG COPPER
3.0U MG/KG MOLYBDENUM
14 MG/KG NICKEL
80 MG/KG LEAD
12U MG/KG ANTIMONY
12U MG/KG SELENIUM
7.SU MG/KG TIN
4.7 MG/KG STRONTIUM
15U MG/KG TELLURIUM
1600 MG/KG TITANIUM
30U MG/KG THALLIUM
49 MG/KG VANADIUM
19 MG/KG YTTRIUM
77 MG/KG ZINC
NA MG/KG ZIRCONIUM
Winston Salem, NC
0.0SU MG/KG TOTAL MERCURY
23000 MG/KG ALUMINUM
1100 MG/KG MANGANESE
880 MG/KG CALCIUM
3900 MG/KG MAGNESIUM
26000 MG/KG IRON
300U MG/KG SODIUM
4500 MG/KG POTASSIUM
9 % % MOISTURE
EPA -REGION IV SESD, ATHENS, GA
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Terri White
Requester: Jennifer Wendel
Project Leader:
Beginning: 10/29/97 15:35
Ending:
Production Date: 11/26/97 15:31
REANALYSIS OF SAMPLES OF PROJ# 97-0329 WAS PERFO
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc ina/cates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-conflrmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
MEMORANDUM
Date: 11 /14/97
•
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of METALS INORGANIC Sample Analysis
RECEI\/ED
NOV 18 1997
SUPERFUND SECT,ON 97-0328 JOHNSON CONTROLS GLOBE
WINSTON-SALEM, NC
From: Keith Bates f:::.-.d /.> Jc:::::-
To: PAT DEROSA
Thru: QA Office
Attached are the results of analysis of samples collected as part of the subject project. If you have any
questions, please contact me.
ATTACHMENT
'
• •
INORGANIC DATA QUALIFIERS REPORT
Case Number:_,2u5~6~3~3=-----------------
Project Number:_.,9~7~-~0~3~2,,_,,8 ______________ _
Site: Johnson Controls Globe, Winston-Salem, NC
Element
A. Waters
Cr, cu
Al, Ca, Fe, Mg,
K, Zn
Na
Na
V
Pb
Co
Pb
Mn
Ni
V
B. Soils
Cr, Cu
Al, Ca, Fe, Mg,
K, Zn
Pb
Se
Flag
u
u
J
J
u
J
J
J
J
J
J
u
u
JN
JN
Samples Affected
All positives> IDL, but
< CRDL
All positives> IDL, but
< CRDL
12453, 12457, 12458, 12459,
12460, 12461
12412, 12415, 12416, 12419,
12420, 12422, 12423, 12425,
12427, 12429, 12431, 12434,
12436, 12438, 12441, 12442,
12447, 12449, 12451
12412, 12416, 12429, 12438,
12442
12416
12434, 12448
12419, 12420
12457
12420, 12423, 12425, 12438,
12441, 12447, 12448, 12451
12419, 12420, 12423, 12425,
12427, 12441, 12447, 12451
12458
All positives> IDL, but
< CRDL
All positives> IDL, but
< CRDL
12413, 12417, 12435
12413, 12435
Reason
Baseline instability
Positives in blanks
Serial dilution percent difference=
14.6%
serial dilution percent difference
10.1%
% RSD > 20% for ICP multiple exposures
and results> IDL, but< CRDL
% RSD > 20% for ICP multiple
exposures
Only analysis of 2X CRDL
required by contract SOW
analysis
Only analysis of 2X CRDL
required by contract sow
analysis
Only analysis of 2X CRDL
required by contract SOW
analysis
standard
for ICP
standard
for ICP
standard
for ICP
Only analysis
required by
analysis
of 2X CRDL standard
contract sow for ICP
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Baseline instability
Positives in blanks
Suspected positive interference as
noted in the contractor res
Suspected positive interference as
noted in the contractor res
• •
INORGANIC DATA QUALIFIERS REPORT (continued)
Case Number: ,15633
Project Number: 97-03,lS
Site: Johnson Controls Globe, Winston-Salem,
Element Flag Samples Affected
Na J 12413, 12414, 12417,
12421, 12424, 12426,
12430, 12432, 12433,
12437, 12439, 12440,
12444, 12445, 12446,
12450, 12452, 12454,
12456
Cr J 12448, 12450, 12452,
12455, 12456
Zn J 12448, 12450, 12452,
12455, 12456
Sb u 12456
As u 12439
Ag u 12418
Tl u 12417, 12418, 12421,
As J 12414, 12433, 12444,
Se J 12 414, 12440, 12444
Tl J 12456
Sb J 12413, 12414, 12417,
12424, 12433, 12435,
12444, 12445, 12446,
As J 12448
Be J 12421, 12424, 12426,
12430, 12432, 12433,
12437, 12439, 12 4 4 0,
12444, 12445, 12446,
12450, 12452, 12454,
12456
NC
12418,
12428,
12435,
12443,
12448,
12455,
12454,
12454,
12440
12456
12418,
12439,
12428,
12435,
12443,
12448,
12455,
Reason
Bliild spike recovery> action limit
Serial dilution percent difference=
12. 6%
Serial dilution percent difference
20. 5%
% RSD > 20% for ICP multiple exposures
and results> IDL, but< CRDL
% RSD > 20% for ICP multiple exposures
and results> IDL, but< CRDL
% RSD > 20% for ICP multiple exposures
and results> IDL, but< CRDL
% RSD > 20% for ICP multiple exposures
and results> IDL, but< CRDL
% RSD > 20% for ICP multiple
exposures
% RSD > 20% for ICP multiple
exposures
% RSD > 20% for ICP rnul tiple
exposures
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Only analysis
required by
analysis
of 2X CRDL standard
contract SOW for ICP
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
•
INORGANIC DATA QUALIFIERS REPORT (continued)
Case Number:_,2~5~6~3~3"'---------------'----
Project Number:_,,9~7c.c:.,0~3~2"'-"8 ______________ _
Site: Johnson Controls Globe, Winston-Salem, NC
Element Flaa
Co J
Ni J
Se J
Ag J
Tl J
Samples Affected
12414, 12421, 12424, 12428,
12430, 12432, 12433, 12435,
12437, 12439, 12440, 12443,
12444, 12450, 12452, 12454,
12455
12424, 12426, 12428, 12432,
12435, 12439, 12444, 12446,
12450, 12452, 12454, 12455
12414, 12440, 12444
12417, 12426, 12445
12413, 12414, 12424, 12433,
12445
Reason
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Only analysis of 2X CRDL st.andard
required by contract SOW for ICP
analysis
Only.analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Only analysis of 2X CRDL standard
required by contract sow for r,cp
analysis
METALS SAMPLE ANALYSIS
Sample 12459 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC001FB MD Number: MP82 lnorg Contractor: CHEM
Media: WATER
RESULTS UNITS ANALYTE
2U UG/L SILVER
7U UG/L ARSENIC
1U UG/L BARIUM
1U UG/L BERYLLIUM
1U UG/L CADMIUM
2U UG/L COBALT
1U UG/L CHROMIUM
1U UG/L COPPER
1U UG/L NICKEL
2U UG/L LEAD
SU UG/L ANTIMONY
SU UG/L SELENIUM
6U UG/L THALLIUM
1U UG/L VANADIUM
2U UG/L ZINC
0.20U UG/L TOTAL MERCURY
40U UG/L ALUMINUM
1U UG/L MANGANESE
30U UG/L CALCIUM
23U UG/L MAGNESIUM
22U UG/L IRON
40J UG/L SODIUM
30U UG/L POTASSIUM
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:45
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actuat value is known to be less than value given. L-actual value is known to be greater than value given. U-material waS analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value ls reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12460 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC001PB MD Number: MP83 lnorg Contractor: CHEM
Media: WATER
RES UL TS UNITS ANALYTE
2U UG/L SILVER
?U UG/L ARSENIC
1U UG/L BARIUM
1U UG/L BERYLLIUM
1U UG/L CADMIUM
2U UG/L COBALT
1U UG/L CHROMIUM
1U UG/L COPPER
1U UG/L NICKEL
2U UG/L LEAD
SU UG/L ANTIMONY
SU UG/L SELENIUM
6U UG/L THALLIUM
1U UG/L VANADIUM
2U UG/L ZINC
0.20U UG/L TOTAL MERCURY
40U UG/L ALUMINUM
1U UG/L MANGANESE
12U UG/L CALCIUM
23U UG/L MAGNESIUM
22U UG/L IRON
27UJ UG/L SODIUM
19U UG/L POTASSIUM
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 14:00
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported. see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12461 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC002PB MD Number: MP84 lnorg Contractor: CHEM
Media: WATER
RESULTS UNITS ANALYTE
2U UG/L SILVER
7U UG/L ARSENIC
1U UG/L BARIUM
1U UG/L BERYLLIUM
1U UG/L CADMIUM
2U UG/L COBALT
1U UG/L CHROMIUM
1U UG/L COPPER
1U UG/L NICKEL
2U UG/L LEAD
5U UG/L ANTIMONY
5U UG/L SELENIUM
6U UG/L THALLIUM
1U UG/L VANADIUM
2U UG/L ZINC
0.20U UG/L TOTAL MERCURY
30U UG/L ALUMINUM
1U UG/L MANGANESE
12U UG/L CALCIUM
23U UG/L MAGNESIUM
22U UG/L IRON
27UJ UG/L SODIUM
19U UG/L POTASSIUM
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 21 :20
Ending:
Production Date: 11/14/97 07:34
A~average value. NA-not analyzed. NAJ-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12455 FY 1997
METALS SCAN
EPA-REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC011SL MD Number: MP66
Media: SOIL
RESULTS
0.54U
2.8
91
0.77J
0.27U
9.6J
22J
15
9.6J
32
1.3U
1.3U
1.6U
48
44J
0.13U
22000
480
870
1700
24000
140J
1500
25
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MP66
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
I norg Contractor: CH EM
Org Contractor: COMPU
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 16:25
Ending:
Production Date: 11/14/97 07:34
~ A-average value. NA-not a-nalyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
METALS SAMPLE ANALYSIS
Sample 12456 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC012SL
Media: SOIL
RESULTS UNITS
0.56U MG/KG
3.3J MG/KG
120 MG/KG
1.1J MG/KG
0.28U MG/KG
18 MG/KG
35J MG/KG
31 MG/KG
19 MG/KG
51 MG/KG
2U MG/KG
1.4U MG/KG
3J MG/KG
79 MG/KG
200J MG/KG
0.14U MG/KG
32000 MG/KG
1100 MG/KG
1400 MG/KG
3300 MG/KG
40000 MG/KG
190J MG/KG
3500 MG/KG
31 %
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: MP67
D Number: MP67
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-nOt aO'atyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/9717:56
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12444 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC013SL MD Number: MP54
Media: SOIL
RES UL TS UNITS
0.49U
2J
68
0.72J
2.2
7.7J
31
15
8.7J
120
2J
1.5J
1.5U
47
250
0.13U
20000
260
670
2300
23000
130J
2400
21
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MP54
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COM PU
· -A-avefage· value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08113197 11 :50
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12445 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC014SL
Media: SOIL
RESULTS UNITS
0.53J MG/KG
1.7U MG/KG
84 MG/KG
0.91J MG/KG
0.25U MG/KG
14 MG/KG
38 MG/KG
25 MG/KG
16 MG/KG
190 MG/KG
2.4J MG/KG
1.2U MG/KG
1.5J MG/KG
51 MG/KG
72 MG/KG
0.12U MG/KG
20000 MG/KG
560 MG/KG
720 MG/KG
3000 MG/KG
25000 MG/KG
180J MG/KG
2800 MG/KG
18 %
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: MP55
D Number: MP55
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 15:45
Ending:
Production Date: 11/14/97 07:34
A-pverage value. NA-not-analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12442 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC001 SW MD Number: MP52
Media: SURFACEWA
RES UL TS UNITS
2U UG/L
7U UG/L
41 UG/L
1 U UG/L
1 U UG/L
2U UG/L
1U UG/L
5U UG/L
1U UG/L
2U UG/L
5U UG/L
5U UG/L
6U UG/L
2U UG/L
7U UG/L
0.20U UG/L
160U UG/L
33 UG/L
6900 UG/L
2500 UG/L
340 UG/L
5400J UG/L
1400 UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MP52
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :00
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the numb-er is the minimum quantitation limit.
R..qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 11/14/97 07:34
Sample 12443 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC001 SD
Media: SEDIM
RESULTS UNITS
0.70U MG/KG
2.5U MG/KG
120 MG/KG
1.3J MG/KG
0.35U MG/KG
12J MG/KG
31 MG/KG
25 MG/KG
15 MG/KG
24 MG/KG
1.8U MG/KG
1.8U MG/KG
2.1U MG/KG
48 MG/KG
71 MG/KG
0.17U MG/KG
20000 MG/KG
490 MG/KG
1200 MG/KG
4400 MG/KG
22000 MG/KG
190J MG/KG
4400 MG/KG
44 %
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: MP53
D Number: MP53
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
. _ A-average value. NA-nOt analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :30
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R--qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12447 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC002SW
Media: SURFACEWA
RESULTS UNITS
2U UG/L
7U UG/L
17 UG/L
1U UG/L
1U UG/L
2U UG/L
5U UG/L
4U UG/L
3J UG/L
2U UG/L
5U UG/L
5U UG/L
6U UG/L
4J UG/L
SU UG/L
0.20U UG/L
780U UG/L
500 UG/L
6400 UG/L
2400 UG/L
1800 UG/L
4100J UG/L
1800 UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: MP57
D Number: MP57
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-aVe"rage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:45
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
METALS SAMPLE ANALYSIS
Sample 12446 FY 1997
METALS SCAN
EPA-REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC002SD MD Number: MP56
Media: SEDIM D Number: MP56
RESULTS UNITS ANALYTE
3.8 MG/KG SILVER
2U MG/KG ARSENIC
160 MG/KG BARIUM
0.76J MG/KG BERYLLIUM
0.29U MG/KG CADMIUM
21 MG/KG COBALT
21 MG/KG CHROMIUM
15 MG/KG COPPER
9.5J MG/KG NICKEL
25 MG/KG LEAD
1.9J MG/KG ANTIMONY
3.1 MG/KG SELENIUM
1.8U MG/KG THALLIUM
33 MG/KG VANADIUM
91 MG/KG ZINC
0.13U MG/KG TOTAL MERCURY
14000 MG/KG ALUMINUM
5600 MG/KG MANGANESE
920 MG/KG CALCIUM
2000 MG/KG MAGNESIUM
21000 MG/KG IRON
130J MG/KG SODIUM
1800 MG/KG POTASSIUM
32 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 12:30
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12448 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC003SD MD Number: MP58
Media: SEDIM
RESULTS UNITS
0.51U
2J
69
0.62J
0.26U
5.9J
16J
9.2
6.7J
52
1.3U
1.3U
1.5U
24
49J
0.13U
7000
460
460
2000
13000
110J
2000
25
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MP58
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
%MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11: 15
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12449 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC004SW
Media: SURFACEWA
RES UL TS UNITS
2U UG/L
7U UG/L
36 UG/L
1U UG/L
1U UG/L
2U UG/L
1U UG/L
5U UG/L
1U UG/L
22 UG/L
5U UG/L
5U UG/L
6U UG/L
1U UG/L
20U UG/L
0.20U UG/L
200U UG/L
270 UG/L
5200 UG/L
2500 UG/L
630 UG/L
6700J UG/L
1700 UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: MP59
D Number: MP59
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
-~-A=-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 10:05
Ending:
Production Date: 11/14197 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12450 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC004SD MD Number: MP60
Media: SEDIM
RESULTS
0.61U
2.1U
88
0.91J
0.30U
6.4J
29J
15
10J
340
1.5U
1.5U
1.8U
36
56J
0.14U
13000
140
920
2900
13000
160J
2600
35
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MP60
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
· A-average va!Ue. -NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/9710:30
Ending:
Production Date: 11/14/97 07:34
K-actua1 value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA Production Date: 11/14/97 07:34
Sample 12451 FY 1997 Project: 97--0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC005SW MD Number: MP61
Media: SURFACEWA D Number: MP61
RESULTS UNITS ANALYTE
2U UG/L SILVER
7U UG/L ARSENIC
33 UG/L BARIUM
1U UG/L BERYLLIUM
1U UG/L CADMIUM
2U UG/L COBALT
1U UG/L CHROMIUM
7U UG/L COPPER
1J UG/L NICKEL
2U UG/L LEAD
5U UG/L ANTIMONY
SU UG/L SELENIUM
6U UG/L THALLIUM
6J UG/L VANADIUM
SU UG/L ZINC
0.20U UG/L TOTAL MERCURY
590U UG/L ALUMINUM
24 UG/L MANGANESE
6400 UG/L CALCIUM
2100 UG/L MAGNESIUM
850 UG/L IRON
7200J UG/L SODIUM
1300 UG/L POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 12:05
Ending:
A-average value. NA:..not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems; 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12452 FY 1997
METALS SCAN
EPA-REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC005SD
Media: SEDIM
RESULTS UNITS
0.56U MG/KG
2U MG/KG
38 MG/KG
0.60J MG/KG
0.28U MG/KG
2.9J MG/KG
17J MG/KG
8 MG/KG
6.1J MG/KG
7.4 MG/KG
1.4U MG/KG
1.4U MG/KG
1.7U MG/KG
15 MG/KG
18J MG/KG
0.14U MG/KG
5100 MG/KG
51 MG/KG
880 MG/KG
1100 MG/KG
4900 MG/KG
120J MG/KG
650 MG/KG
30 %
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: MP62
D Number: MP62
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 12:35
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12422 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC006SW
Media: SURFACEWA
RESULTS
2U
7U
32
1U
1U
2U
1U
4U
1U
5
5U
5U
6U
1U
7U
0.20U
210U
360
5700
2300
2600
5500J
1400
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: MH94
D Number: MH94
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estirnated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 12:25
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12423 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC106SW MD Number: MH95
Media: SURFACEWA D Number: MH95
RESULTS UNITS ANALYTE
2U UG/L SILVER
7U UG/L ARSENIC
32 UG/L BARIUM
1U UG/L BERYLLIUM
1U UG/L CADMIUM
2U UG/L COBALT
4U UG/L CHROMIUM
4U UG/L COPPER
3J UG/L NICKEL
5 UG/L LEAD
5U UG/L ANTIMONY
5U UG/L SELENIUM
6U UG/L THALLIUM
1J UG/L VANADIUM
20U UG/L ZINC
0.20U UG/L TOTAL MERCURY
200U UG/L ALUMINUM
350 UG/L MANGANESE
5600 UG/L CALCIUM
2300 UG/L MAGNESIUM
2500 UG/L IRON
5400J UG/L SODIUM
1300 UG/L POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 12:30
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12424 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97 -0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC006SD
Media: SEDIM
RESULTS UNITS
1.6U MG/KG
5.6U MG/KG
240 MG/KG
2.1J MG/KG
0.80U MG/KG
26J MG/KG
60 MG/KG
49 MG/KG
30J MG/KG
300 MG/KG
5J MG/KG
4U MG/KG
64J MG/KG
93 MG/KG
130 MG/KG
0.38U MG/KG
50000 MG/KG
1400 MG/KG
1800 MG/KG
4200 MG/KG
73000 MG/KG
250J MG/KG
3400 MG/KG
76 %
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: MH96
D Number: MH96
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 13:00
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R--qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12434 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC007SW
Media: SURFACEWA
RES UL TS UNITS
2U UG/L
7U UG/L
74 UG/L
1U UG/L
1U UG/L
2J UG/L
1U UG/L
3U UG/L
1U UG/L
2U UG/L
SU UG/L
SU UG/L
6U UG/L
1U UG/L
20U UG/L
0.20U UG/L
120U UG/L
1700 UG/L
8500 UG/L
2600 UG/L
16000 UG/L
4000J UG/L
1400 UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: MK09
D Number: MK09
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:26
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12436 FY 1997
METALS SCAN
EPA-REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC107SW MD Number: MK11
Media: SURFACEWA D Number: MK11
RESULTS UNITS ANALYTE
2U UG/L SILVER
7U UG/L ARSENIC
72 UG/L BARIUM
1U UG/L BERYLLIUM
1U UG/L CADMIUM
2U UG/L COBALT
1U UG/L CHROMIUM
1U UG/L COPPER
1U UG/L NICKEL
2U UG/L LEAD
5U UG/L ANTIMONY
5U UG/L SELENIUM
6U UG/L THALLIUM
1U UG/L VANADIUM
9U UG/L ZINC
0.20U UG/L TOTAL MERCURY
90U UG/L ALUMINUM
1600 UG/L MANGANESE
8300 UG/L CALCIUM
2500 UG/L MAGNESIUM
15000 UG/L IRON
3900J UG/L SODIUM
1300 UG/L POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyze·d. NAl-interferences. J--estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:26
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12435 FY 1997
METALS SCAN
EPA-REGION IV SESD, ATHENS., GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC007SD MD Number: MK10
Media: SEDIM
RES UL TS UNITS
0.93U
5.9
170
1.7J
0.46U
14J
40
31
18J
34JN
5.1J
2.7JN
2.8U
73
97
1.1
43000
550
1200
2800
71000
200J
2200
69
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MK10
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:55
Ending:
Production Date: 11/14/97 07:34
K-actua1 value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R--qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12438 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC00BSW MD Number: MK13
Media: SURFACEWA
RESULTS UNITS
2U UG/L
7U UG/L
24 UG/L
1U UG/L
1U UG/L
2U UG/L
4U UG/L
3U UG/L
3J UG/L
2U UG/L
5U UG/L
5U UG/L
6U UG/L
2U UG/L
6U UG/L
0.20U UG/L
190U UG/L
350 UG/L
6000 UG/L
2400 UG/L
1300 UG/L
4500J UG/L
1400 UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MK13
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 19:25
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12437 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC008SD MD Number: MK12
Media: SEDIM D Number: MK12
RESULTS UNITS ANALYTE
0.67U MG/KG SILVER
2.4U MG/KG ARSENIC
120 MG/KG BARIUM
1.3J MG/KG BERYLLIUM
0.34U MG/KG CADMIUM
13J MG/KG COBALT
34 MG/KG CHROMIUM
20 MG/KG COPPER
14 MG/KG NICKEL
15 MG/KG LEAD
1.7U MG/KG ANTIMONY
1.7U MG/KG SELENIUM
2U MG/KG THALLIUM
52 MG/KG VANADIUM
69 MG/KG ZINC
0.16U MG/KG TOTAL MERCURY
26000 MG/KG ALUMINUM
570 MG/KG MANGANESE
1100 MG/KG CALCIUM
3300 MG/KG MAGNESIUM
26000 MG/KG IRON
180J MG/KG SODIUM
2800 MG/KG POTASSIUM
42 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
A:ave/"age value.-NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number ls the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12439 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC108SD MD Number: MK14
Media: SEDIM
RESULTS UNITS
0.65U
3U
110
1.2J
0.32U
11J
30
19
12J
14
2J
1.6U
1.9U
47
62
0.16U
21000
520
910
2900
23000
170J
2400
39
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MK14
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolltes of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12441 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC009SW MD Number: MP51
Media: SURFACEWA
RES UL TS UNITS
2U UG/L
7U UG/L
27 UG/L
1U UG/L
1U UG/L
2U UG/L
15 UG/L
20U UG/L
BJ UG/L
2U UG/L
5U UG/L
5U UG/L
6U UG/L
1J UG/L
5U UG/L
0.34 UG/L
230 UG/L
370 UG/L
6400 UG/L
2600 UG/L
1800 UG/L
5300J UG/L
1500 UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MP51
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value.-NA-not·analyzed. ·NAl-interferences. J-estima!ed value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:45
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12440 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC009SD MD Number: MP50
Media: SEDIM
RESULTS
0.80U
2.8U
160
1.9J
0.40U
18J
49
28
21
22
4U
2.3J
4U
74
100
0.21U
38000
930
1300
4000
40000
250J
3400
53
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MP50
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:30
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12453 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC010SW MD Number: MP63
Media: SURFACEWA D Number: MP63
RESULTS UNITS ANALYTE
2U UG/L SILVER
7U UG/L ARSENIC
30 UG/L BARIUM
1U UG/L BERYLLIUM
1U UG/L CADMIUM
2U UG/L COBALT
1U UG/L CHROMIUM
1U UG/L COPPER
1U UG/L NICKEL
2U UG/L LEAD
5U UG/L ANTIMONY
5U UG/L SELENIUM
6U UG/L THALLIUM
1U UG/L VANADIUM
2U UG/L ZINC
0.20U UG/L TOTAL MERCURY
60U UG/L ALUMINUM
34 UG/L MANGANESE
4900 UG/L CALCIUM
2300 UG/L MAGNESIUM
210U UG/L IRON
2500J UG/L SODIUM
1000 UG/L POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 09:40
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation timit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirrned by gems: 1.when no value is reported, see chlordane constituents 2.constituents or me-tabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA
Sample 12454 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC01 0SD MD Number: MP64
Media: SEDIM
RESULTS UNITS
0.52U
1.8U
80
1J
0.26U
8.1J
25J
9.7
7.8J
6.8
1.3U
1.3U
1.6U
31
25J
0.14U
8500
240
550
1700
13000
130J
1200
26
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MP64
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 09:25
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESO, ATHENS, GA
Sample 12429 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, .NC
Program: NSF
Id/Station: JC011 SW
Media: SURFACEWA
RESULTS
2U
7U
29
1U
1U
2U
1U
4U
1U
2U
SU
SU
6U
2U
SU
0.20U
180U
23
5900
3000
560
3800J
1000
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: MJ01
D Number: MJ01
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
I norg Contractor: CH EM
Org Contractor: COMPU
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:25
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NA1-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA
Sample 12430 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC011 SD MD Number: MJ02
Media: SEDIM
RESULTS UNITS
0.74U
2.6U
93
0.91J
0.37U
12J
39
23
16
11
1.8U
1.8U
2.2U
52
42
0.17U
18000
260
1100
2500
23000
200J
1700
46
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MJ02
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
%MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
Production Date: 11/14/97 07:34
A-civerage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12420 FY 1997
METALS SCAN
EPA-REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Stalion:JC012SW MD Number: MH92
Media: SURFACEWA
RESULTS UNITS
2U UG/L
7U UG/L
23 UG/L
1U UG/L
1U UG/L
2U UG/L
29 UG/L
9U UG/L
15J UG/L
3J UG/L
SU UG/L
SU UG/L
6U UG/L
1J UG/L
9U UG/L
0.20U UG/L
150U UG/L
330 UG/L
5800 UG/L
2400 UG/L
1400 UG/L
4700J UG/L
1300 UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MH92
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/9711:12
Ending:
Production Date: 11/14/97 07:34
· A-average Value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12421 FY 1997
METALS SCAN
EPA-REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC012SD
Media: SEDIM
RESULTS UNITS
0.60U MG/KG
2.1U MG/KG
140 MG/KG
1.3J MG/KG
0.30U MG/KG
14J MG/KG
37 MG/KG
17 MG/KG
15 MG/KG
16 MG/KG
3U MG/KG
1.5U MG/KG
3U MG/KG
56 MG/KG
69 MG/KG
0.14U MG/KG
25000 MG/KG
470 MG/KG
730 MG/KG
4200 MG/KG
28000 MG/KG
170J MG/KG
3800 MG/KG
35 %
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: MH93
D Number: MH93
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 11 :30
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12431 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC013SW
Media: SURFACEWA
RESULTS
2U
7U
22
1U
1U
2U
1U
4U
1U
2U
5U
5U
6U
1U
3U
0.20U
90U
37
5900
3000
360
4500J
1200
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: MK06
D Number: MK06
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:35
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12432 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC013SD MD Number: MK07
Media: SEDIM D Number: MK07
RESULTS UNITS ANALYTE
0.59U MG/KG SILVER
2.1U MG/KG ARSENIC
57 MG/KG BARIUM
0.55J MG/KG BERYLLIUM
0.29U MG/KG CADMIUM
6.7J MG/KG COBALT
16 MG/KG CHROMIUM
11 MG/KG COPPER
7.3J MG/KG NICKEL
4.7 MG/KG LEAD
1.5U MG/KG ANTIMONY
1.5U MG/KG SELENIUM
1.8U MG/KG THALLIUM
22 MG/KG VANADIUM
20 MG/KG ZINC
0.13U MG/KG TOTAL MERCURY
9400 MG/KG ALUMINUM
360 MG/KG MANGANESE
550 MG/KG CALCIUM
1400 MG/KG MAGNESIUM
11000 MG/KG IRON
130J MG/KG SODIUM
890 MG/KG POTASSIUM
32 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
· A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:50
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actuat value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampllng and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12419 FY 1997
METALS SCAN
EPA· REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC014SW MD Number: MH91
Media: SURFACEWA
RESULTS UNITS
2U UG/L
7U UG/L
50 UG/L
1U UG/L
1U UG/L
2U UG/L
1U UG/L
4U UG/L
1 U UG/L
2J UG/L
5U UG/L
5U UG/L
6U UG/L
3J UG/L
ZOU UG/L
0.20U UG/L
380U UG/L
140 UG/L
7300 UG/L
3300 UG/L
1300 UG/L
4800J UG/L
3200 UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MH91
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:45
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12418 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC014SD MD Number: MH90
Media: SEDIM
RESULTS
1U
4.5
230
2.3
0.40U
24
70
30
32
22
2.4J
2.3
5U
80
84
0.23U
34000
950
3600
6800
37000
270J
5000
56
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MH90
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value.·NA-not analyzed. -NA.I-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:33
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be Jess than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12427 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC015SW
Media: SURFACEWA
RESULTS UNITS
2U UG/L
7U UG/L
39 UG/L
1U UG/L
1U UG/L
2U UG/L
1U UG/L
SU UG/L
1U UG/L
2U UG/L
SU UG/L
SU UG/L
6U UG/L
1J UG/L
6U UG/L
0.20U UG/L
300U UG/L
130 UG/L
7200 UG/L
3400 UG/L
2700 UG/L
3900J UG/L
1300 UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: MH99
D Number: MH99
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 11:47
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interfererices. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane ·
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12428 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC015SD MD Number: MJ00
Media: SEDIM
RESULTS
0.71U
2.5U
110
1.1J
0.35U
11J
33
19
12J
18
1.8U
1.8U
2.1U
47
63
0.17U
23000
590
1200
2100
30000
200J
1600
45
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MJ00
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/9712:15
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R--qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12433 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC016SD MD Number: MK0B
Media: SEDIM
RESULTS
0.92U
5U
180
2.1J
0.46U
17J
48
41
24
45
3J
2.3U
3.3J
98
82
0.29U
50000
760
1200
3200
40000
. 190J
2800
69
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MK0B
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 15:35
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12425 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC017SW MD Number: MH97
Media: SURFACEWA
RESULTS
2U
7U
33
1U
1U
2U
6U
BU
4J
2U
SU
SU
6U
1J
SU
0.20U
160U
17
7800
3600
320
4300J
1200
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MH97
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:30
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirrned by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12426 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC017SD
Media: SEDIM
RESULTS UNITS
0.78J MG/KG
1.9U MG/KG
42 MG/KG
0.68J MG/KG
0.26U MG/KG
20 MG/KG
52 MG/KG
15 MG/KG
10J MG/KG
7.7 MG/KG
2U MG/KG
1.3U MG/KG
1.6U MG/KG
70 MG/KG
18 MG/KG
0.12U MG/KG
10000 MG/KG
820 MG/KG
580 MG/KG
680 MG/KG
22000 MG/KG
110J MG/KG
430 MG/KG
24 %
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: MH98
D Number: MH98
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:40
Ending:
Production Date: 11/14/97 07:34
A-average value-. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-materia1 was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12412 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC018SW
Media: SURFACEWA
RESULTS
2U
7U
26
1U
1U
1U
1U
SU
1U
4
SU
SU
6U
2U
40
0.20U
240U
300
6000
2500
2000
4400J
1400
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: LL02
D Number: LL02
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value.-NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 16:32
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12413 FY 1997
METALS SCAN
EPA -REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC018SD MD Number: LL03
Media: SEDIM
RESULTS UNITS
0.79U
5.1
230
2.6
0.40U
22
63
42
27
47JN
3.2J
2.8JN
3J
110
130
0.27U
56000
630
1700
5000
44000
300J
4200
63
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: LL03
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
. -A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 17:35
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value ls reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12414 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC019SD MD Number: LL04
Media: SEDIM D Number: LL04
RESULTS UNITS ANALYTE
a.sou MG/KG SILVER
4.4J MG/KG ARSENIC
200 MG/KG BARIUM
2.2 MG/KG BERYLLIUM
0.40U MG/KG CADMIUM
19J MG/KG COBALT
55 MG/KG CHROMIUM
33 MG/KG COPPER
24 MG/KG NICKEL
38 MG/KG LEAD
3.3J MG/KG ANTIMONY
3J MG/KG SELENIUM
2.SJ MG/KG THALLIUM
94 MG/KG VANADIUM
110 MG/KG ZINC
0.21U MG/KG TOTAL MERCURY
49000 MG/KG ALUMINUM
530 MG/KG MANGANESE
1500 MG/KG CALCIUM
4500 MG/KG MAGNESIUM
40000 MG/KG IRON
260J MG/KG SODIUM
3700 MG/KG POTASSIUM
57 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
-A-aVeraQe value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 17:50
Ending:
Production Date: 11/14/97 07:34
K-actuaJ value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12415 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC020SW MD Number: LL05
Media: SURFACEWA
RESULTS UNITS
2U UG/L
7U UG/L
14 UG/L
1U UG/L
1U UG/L
2U UG/L
1U UG/L
7U UG/L
1U UG/L
2U UG/L
5U UG/L
5U UG/L
6U UG/L
1U UG/L
26 UG/L
0.20U UG/L
90U UG/L
45 UG/L
5700 UG/L
2300 UG/L
180U UG/L
5000J UG/L
1600 UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: LL05
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 15:00
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12416 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC021 SW
Media: SURFACEWA
RESULTS
2U
7U
24
1U
1U
2U
1U
5U
1U
4J
5U
5U
6U
2U
20U
0.20U
180U
150
7200
2800
1200
6800J
1800
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: LL06
D Number: LL06
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 17:00
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12417 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC021 SD MD Number: MH89
Media: SEDIM D Number: MH89
RESULTS UNITS ANALYTE
0.94J MG/KG SILVER
4.9 MG/KG ARSENIC
270 MG/KG BARIUM
2.2 MG/KG BERYLLIUM
0.40U MG/KG CADMIUM
24 MG/KG COBALT
62 MG/KG CHROMIUM
47 MG/KG COPPER
30 MG/KG NICKEL
46JN MG/KG LEAD
4J MG/KG ANTIMONY
2U MG/KG SELENIUM
4U MG/KG THALLIUM
100 MG/KG VANADIUM
130 MG/KG ZINC
0.25U MG/KG TOTAL MERCURY
66000 MG/KG ALUMINUM
490 MG/KG MANGANESE
1400 MG/KG CALCIUM
5100 MG/KG MAGNESIUM
64000 MG/KG IRON
350J MG/KG SODIUM
4300 MG/KG POTASSIUM
62 % % MOISTURE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 18:40
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12457 FY 1997 Project: 97-0328
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC001 PW
Media: GROUNDWA
RESULTS
2U
7U
31
1U
1U
2U
1U
490
1U
11
5U
5U
6U
1U
100
0.20U
50U
BJ
2300
1300
30U
3000J
890
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
Case Number: 25633
MD Number: MP68
D Number: MP68
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: Keith Bates
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:15
Ending:
Production Date: 11/14/97 07:34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS
Sample 12458 FY 1997
METALS SCAN
EPA-REGION IV SESD, ATHENS, GA
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC002PW MD Number: MP69
Media: GROUNDWA
RESULTS UNITS
2U UG/L
7U UG/L
8 UG/L
1U UG/L
1U UG/L
2U UG/L
1U UG/L
20U UG/L
1U UG/L
2U UG/L
5U UG/L
5U UG/L
6U UG/L
1J UG/L
26 UG/L
0.20U UG/L
40U UG/L
1U UG/L
11000 UG/L
4700 UG/L
SOU UG/L
4900J UG/L
1300 UG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MP69
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 21:00
Ending:
Production Date: 11/14/97 07:34
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R--qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
• •
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
MEMORANDUM
Date: 09/16/97
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of METALS INORGANIC Sample Analysis
97-0329 JOHNSON CONTROLS GLOBE
WINSTON-SALEM, NC
From: Gary Bennettff fa-
To: PAT DEROSA
RECEIVED
SEP 19 1997,
SUPERFUND SECTION
Attached are the results of analysis of samples collected as part of the subject project. If you have any
questions, please contact me.
ATTACHMENT
' '
• •
INORGANIC DATA QUALIFIERS REPORT
Case Number: Johnson Control Globe
Project Number:__,9~7~-~0~3~2"-"9 ____________ _
Site: Johnson Control Globe, Winston-Salem, NC
Element
A. Soils
Sb, Cd, Pb, Se,
Ag
Ba
Be
Cd
Pb
Tl
Sb
As
Ba
Be
Cd
Cr
Co
Cu
Pb
Flag
u
u
JN
JN
JN
J
J
J
R
J
J
J
J
J
J
J
Samples Affected
All positives >IDL, but< CRDL
< CRDL
All positives> IDL, ·but< CRDL
12476, 12479, 12480, 12481, 12482,
12483, 12484
12476, 12479, 12480, 12481, 12482.
12483, 12484, 12485
12476, 12477, 12478, 12479, 12480,
12481, 12482, 12483, 12484, 12485
12476, 12479, 12480, 12481, 12482,
12483, 12484
Reason
Baseline instability
Positives in blanks
Suspected positive interference
as noted in the contractor res
Suspected positive interference
as noted in the contractor res
Suspected positive.interference
as noted in the contractor res
Suspected over correction as
noted in the contractor res
12476, 12477, 12478, 12479, 12480, Matrix spike recovery= 50.2%
12481, 12482, 12483, 12484, 12485
12476, 12477, 12478, 12480, 12481,
12482, 12483, 12485
12479, 12484
12476, 12477, 12478, 12479, 12480,
12481, 12482, 12483, 12484, 12485
12476, 12477, 12478, 12479, 12480,
12481, 12482, 12483, 12484, 12485
Matrix spike recovery= 137.8%
Blind spike recovery< action
limit
Matrix spike recovery= 154.9%
Blind spike recovery< warning
limit
Matrix spike recovery= 154.9%
Blind spike recovery > action
limit
12476, 12477, 12478, 12479, 12480, Matrix spike recovery= 161.2%
12481, 12482, 12483, 12484, 12485
12476, 12477, 12478, 12479, 12480, Matrix spiked recovery
12481, 12482, 12483, 12484, 12485
159.2%
12476, 12477, 12478, 12479, 12480,
12481, 12482, 12483, 12484, 12485
12476, 12477, 12478, 12479, 12480,
12481, 12482, 12483, 12484, 12485
12476, 12477, 12478, 12479, 12480,
12481, 12482, 12483, 12484, 12485
Matrix spike recovery= 152.2%
Blind spike recovery < action
limit
Matrix' spike recovery= 147.4%
Blind spike recovery < actiori
limit
Matrix spike recovery= 136.2%
Blind spike recovery< action
limit
Serial dilution percent
difference= 11.1%
• •
INORGANIC DATA QUALIFIERS REPORT (Continued)
Case Number: Johnson Control Globe
Project Number: ·97-0329
Site: Johnson Control Globe, Winston-Salem, NC
Element J:::J.ag Samgles Af{ected Reason
Ni J 12476, 12477, 124 7 8, 124 7 9, 12480, Matrix spike recovery = 160%
12481, 12482, 12483, 12484, 12485
Ag J 12476, 12477, 12478, 12479, 12480, Matrix spike recovery 152.5%
12481, 12482, 12483, 12484, 12485
V J 12476, 12477, 12478, 124 79, 12480, Matrix spike recovery= 163%
12481, 12482, 12483, 12484, 12485 Blind spike recovery< action
limit
Zn J 12476, 12477, 12478, 12479, 12480, Matrix spike recovery= 148.8%
12481, 12482, 12483, 12484, 12485 Blind spike recovery< action
limit
Seril dilution percent
difference = 19.5%
Al J 12476, 12477, 12478, 12479, 12480, Blind spike recovery< action
12481, 12482, 12483, 12484, 12485 limit
Seril dilution percent
difference = 19.5%
Ca J 12476, 124 77, 12478, 12479, 12480,. Blind spike recovery < action
12481, 12482, 12483, 12484, 12485 lirni t
Seril dilution percent
difference = 15.8%
Fe J 12476, 12477, 12478, 12479, 1248 0, Blind spike recovery < action
12481, 12482, 12483, 12 4 8 4, 12485 limit
Seril dilution percent
difference = 15. 7%
Mg J 12476, 12477, 12478, 12479, 12480, Blind spike recovery< warning
12481, 12482, 1,2483, 12484,. 12485 limit
Seril dilution percent
difference = 17.2%
Mn J 12476, 12477, 12478, 124 79, 12480, Blind spike recovery < action
12 4 81, 12482, 12483, 1248 4, 12485 limit ' ·Seril dilution percent
difference = 16.8%
K J 12476, 12 4 77, 12478, 12479, 12480, Blind spike recovery < action
12481, 12482, 12483, .12484, 12485 limit
As u 12 4 77, 12485 % RSD > 20% for ICP multiple
exposures and results were >
IDL, but < CRDL
Hg J 12476, 12477, 12478, 12479, 1248 0, No instrument printout of data
12481, 12482, 12483, 12484, 12485 included in raw data
• •
INORGANIC DATA QUALIFIERS REPORT (Continued)
Case Number: Johnson Control Globe
Project Number:_,9~7~-~0~3~2"-"9 _____________ _
Site: Johnson Control Globe, Winston-Salem, NC
Element
TCLP Extract
Pb, Se
Ba
Cr
Cr
Pb
. As
Cd
Se
Ag
Cd
Cr
Se
Ag
As
As
Ba
Flag
u
u
J
J
J
u
u
u
u
J
J
J
J
J
J
J
Samples Affected
All positives> IDL, but
< CRDL
All positives> IDL, but
< l0X contaminant level
12476, 12477, 12478, 12479, 12480
12481, 12482, 12483, 12484, 12485
12476, 12477, 12478, 12479, 12480
12481, 12482, 12483, 12484, 12485
12476, 12477, 12478, 12479, 12480,
12481, 12482, 12483, 12484, 12485
12476, 12477
12476, 12477, 12478
12481, 12484
12481, 12483, 12485
12482, 12483, 12484
12479, 12481, 12482, 12483, 12484
12476, 12478, ·12400, 12405
12480, 12484
12479, 12480
12477, 12478, 12479, 12480, 12481
12483, 12484, 12485
12476, 12477, 12478, 12479, 12480
12481; 12482, 12483, 12484, 12485
Reason
Baseline instability
Positives in blanks
Negative with absolute value>
CRDL reported in blank
Matrix duplicate RPD = 200%
Serial dilution percent
difference= 12.7%
% RSD > 20% for ICP multiple
exposures and results > IDL,
but< CRDL
% RSD > 20% foe ICP multiple
exposures and results > IDL,
but< CRDL
% RSO > 20% for ICP multiple
exposures and results > IDL,
but< CRDL
% RSD > 20% for ICP multiple
exposures and results > IDL,
but< CRDL
% RSD > 20% for ICP multiple
exposures
% RSD > 20% for ICP multiple
exposures
·% RSD > 2rn-·for ICP multiple
exposures
% RSD > 20% for ICP multiple
exposures
Only analysis of
standard required by
SOW for ICP analysis
2X CRDL
contract
No extraction blank analyzed by
the laboratory
No extraction blank analyzed by
the laboratory
• •
INORGANIC DATA QUALIFIERS REPORT (Continued)
Case Number: Johnson Control Globe
Project Number:_,9~7=0~3=2~9c_ ____________ _
Site: Johnson Control Globe, Winston-Salem, NC
Element Flag sarngles Affected Reason
Cd J 124 77, 12478, 12479, 12480, 12481 No extraction blank analyzed by
12482, 12483, 12484, 12485 the laboratory
Cr J 12477, 12478, 12479, 12480, 12481 No extraction blank analyzed by
12482, 12483, 12484 the laboratory
Pb J 12476, 12477, 12478, 12479,. 12480 No extraction blank analyzed by
12481, 12482, 12483, 12 4 8 4, 12485 the laboratory
Se J 12476, 12478, 12480, 12481, 12483 No extraction blank analyzed by
12484, 12485 the laboratory
METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA PRINTED 09/16/97 10:41
Sample 12476 FY 1997
METALS SCAN
Project: 97.{)329
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JB01 0SL
Media: SOIL
RES UL TS UNITS
13000J
0.6UJ
0.96J
100J
0.85J
4.1JN
1100J
32J
18J
20J
19000J
26JN
2500J
760J
0.34J
19J
2200J
0.32U
2.6J
54
0.36UJ
51J
370J
23
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
.LEAD
MD Number: MP65
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
A-average·value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 17:20
Ending:
K-actual value is knovm to be less than value given. L-actuaf value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 09/16/97 10:41
Sample 12476 FY 1997
METALS TCLP SCAN
Project: 97 -0329
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JB01 0SL
Media: SOIL
RESULTS
0.007U
0.007U
1.6J
NA
0.003U
0.01UJ
NA
0.022J
NA
O.OOBJ
NA
0.0002IJ
UNITS
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
MD Number: MP65
TOTAL MERCURY
SAS Number:TCLP
lnorg Contractor: ANTEC
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 17:20
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resam.pling and reanalysis is necessary for verification.
C--confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technic_al chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 09/16/97 10:41
Sample 12477 FY 1997 Project: 97-0329
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB001 SL
Media: SOIL
RESULTS
6200J
0.58UJ
1UJ
53J
0.57J
2.3J
490J
20J
9.8J
14J
8700J
16JN
1600J
210J
0.08UJ
10J
1000J
0.31U
2.3J
46
0.36U
25J
32J
14
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
MD Number: MP70
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
A-average value: 'NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 17: 15
Ending:
K-actua1 value is known to be less than value given. L-actual value ls known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituent.s or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA PRINTED 09/16/97 10:41
Sample 12477 FY 1997 Project: 97 -0329
METALS TCLP SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB001 SL
Media: SOIL
MD Number: MP70
RESULTS
0.00?U
0.00BUJ
0.98J
NA
0.005UJ
0.012J
NA
0.012J
NA
0.003U
NA
0.0002U
UNITS
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
TOTAL MERCURY
SAS Number:TCLP
lnorg Contractor: ANTEC
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
.Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 17:15
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound niay or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 09/16/97 10:41
Sample 12478 FY 1997 Project: 97 -0329
METALS TCLP SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB101SL MD Number: MP71
Media: SOIL
RESULTS
0.007U
0.76J
0.92J
NA
0.003UJ
0.025J
NA
0.025J
NA
0.011J
NA
0.0002U
UNITS
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
TOTAL MERCURY
SAS Number:TCLP
lnorg Contractor: ANTEC
A-aVerage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 17:15
Ending:
K-actual value is known to be less than value given. L-actual value is known t6 be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 09/16/97 10:41
Sample 12478 FY 1997 Project: 97 -0329
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
ld/Station:JB101SL MD Number: MP71 lnorg Contractor: ANTEC
Media: SOIL
RESULTS UNITS ANALYTE
6000J MG/KG ALUMINUM
0.64UJ MG/KG ANTIMONY
0.84J MG/KG ARSENIC
65J MG/KG BARIUM
0.61J MG/KG BERYLLIUM
2.2J MG/KG CADMIUM
640J MG/KG CALCIUM
19J MG/KG CHROMIUM
10J MG/KG COBALT
15J MG/KG COPPER
8400J MG/KG IRON
19JN MG/KG LEAD
1600J MG/KG MAGNESIUM
370J MG/KG MANGANESE
0.12UJ MG/KG TOTAL MERCURY
9.7J MG/KG NICKEL
1000J MG/KG POTASSIUM
0.34U MG/KG SELENIUM
2.1J MG/KG SILVER
38 MG/KG SODIUM
0.39U MG/KG THALLIUM
25J MG/KG VANADIUM
30J MG/KG ZINC
15 % % MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 17:15
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reJ)orted, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 09/16/97 10:41
Sample 12479 FY 1997 • Project: 97-0329
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
ld/Station:JB003SL MD Number: MP72 lnorg Contractor: ANTEC
Media: SOIL
RESULTS UNITS ANALYTE
7500J MG/KG ALUMINUM
0.59UJ MG/KG ANTIMONY
0.49UR MG/KG ARSENIC
53J MG/KG BARIUM
0.69JN MG/KG BERYLLIUM
3.4JN MG/KG CADMIUM
1600J MG/KG CALCIUM
26J MG/KG CHROMIUM
10J MG/KG COBALT
21J MG/KG COPPER
16000J MG/KG IRON
7.3JN MG/KG LEAD
4200J MG/KG MAGNESIUM
370J MG/KG MANGANESE
0.09UJ MG/KG TOTAL MERCURY
16J MG/KG NICKEL
1800J MG/KG POTASSIUM
0.32U MG/KG SELENIUM
2.7J MG/KG SILVER
370 MG/KG SODIUM
0.36UJ MG/KG THALLIUM
47J MG/KG VANADIUM
52J MG/KG ZINC
14 % % MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 18:30
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1. when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 09/16/97 10:41
Sample 12479 FY 1997 Project: 97 --0329
METALS TCLP SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JB003SL
Media: SOIL
MD Number: MP72
RESULTS
O.OO?U
0.006J
0.20J
NA
0.004UJ
0.014J
NA
0.008J
NA
0.003U
NA
0.0002U
UNITS
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
TOTAL MERCURY
SAS Number:TCLP
lnorg Contractor: ANTEC
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 18:30
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 09/16/9710:41
Sample 12480 FY 1997
METALS TCLP SCAN
Project: 97-0329
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JB004SL
Media: SOIL
RESULTS
0.012J
0.009J
2.0J
NA
0.009J
0.03J
NA
0.074J
NA
0.007J
NA
0.0002U
UNITS
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
MD Number: MP73
TOTAL MERCURY
SAS Number:TCLP
lnorg Contractor: ANTEC
A~average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 17:45
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituentS or metabolites of technical chlordane
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 09/16/97 10:41
Sample 12480 FY 1997 Project: 97-0329
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JB004SL
Media: SOIL
RESULTS
13000J
0.51UJ
1.3J
83J
0.99J
4.1JN
1200J
27J
13J
29J
20000J
74JN
3100J
650J
0.11 UJ
19J
2100J
0.27U
2.6J
97
0.31UJ
53J
100J
7
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
. MD Number: MP73
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning 08/13/97 17:45
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA PRINTED 09/16/97 10:41
Sample 12481 FY 1997 Project: 97 --0329
METALS TCLP SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
ld/Station:JB005SL MD Number: MP74 lnorg Contractor: ANTEC
Media: SOIL
RESULTS UNITS ANALYTE
0.01 UJ MG/L SILVER
0.013J MG/L ARSENIC
1 03J MG/L BARIUM
NA MG/L BERYLLIUM
0.00?J MG/L CADMIUM
0.018J MG/L CHROMIUM
NA MG/L NICKEL
0.012J MG/L LEAD
NA MG/L ANTIMONY
0.004UJ MG/L SELENIUM
NA MG/L THALLIUM
0.0002U MG/L TOTAL MERCURY
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 19:00
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA-REGION JV SESD, ATHENS, GA PRINTED 09/16/97 10:41
Sample 12481 FY 1997 Project: 97--0329
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
ld/Station:JB005SL MD Number: MP74 lnorg Contractor: ANTEC
Media: SOIL
RESULTS UNITS ANALYTE
14000J MG/KG ALUMINUM
0.52UJ MG/KG ANTIMONY
1.5J MG/KG ARSENIC
76J MG/KG BARIUM
0.64JN MG/KG BERYLLIUM
4.2JN MG/KG CADMIUM
4500J MG/KG CALCIUM
28J MG/KG CHROMIUM
8.8J MG/KG COBALT
27J MG/KG COPPER
20000J MG/KG IRON
18JN MG/KG LEAD
3300J MG/KG MAGNESIUM
270J MG/KG MANGANESE
0.11 UJ MG/KG TOTAL MERCURY
14J MG/KG NICKEL
2900J MG/KG POTASSIUM
0.28U MG/KG SELENIUM
2.4J MG/KG SILVER
98 MG/KG SODIUM
0.32UJ MG/KG THALLIUM
52J MG/KG VANADIUM
54J MG/KG ZINC
12 % % MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 19:00
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 09/16/97 10:41
Sample 12482 FY 1997 Project: 97--0329
METALS TCLP SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JB006SL
Media: SOIL
MD Number: MP75
RESULTS
0.007U
0.005U
1.2J
NA
0.012J
0.012J
NA
7.1J
NA
0.003U
NA
0.0002U
UNITS
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
TOTAL MERCURY
SAS Number:TCLP
lnorg Contractor: ANTEC
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 19:00
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA PRINTED 09/16/97 10:41
Sample 12482 FY 1997
METALS SCAN
Project: 97 -0329
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB006SL MD Number: MP75
Media: SOIL
RESULTS UNITS ANALYTE
15000J MG/KG ALUMINUM
0.78UJ MG/KG ANTIMONY
2.2J MG/KG ARSENIC
82J MG/KG BARIUM
0.95JN MG/KG BERYLLIUM
5.3JN MG/KG CADMIUM
4700J MG/KG CALCIUM
36J MG/KG CHROMIUM
14J MG/KG COBALT
62J MG/KG COPPER
26000J MG/KG IRON
2000JN MG/KG LEAD
3500J MG/KG MAGNESIUM
510J MG/KG MANGANESE
0.15UJ MG/KG TOTAL MERCURY
23J MG/KG NICKEL
2300J MG/KG POTASSIUM
0.42U MG/KG SELENIUM
3.5J MG/KG SILVER
820 MG/KG SODIUM
0.47UJ MG/KG THALLIUM
68J MG/KG VANADIUM
180J MG/KG ZINC
38 % % MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
A-average value. NA~not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning: 08113/97 19:00
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-con_firmed by gems: 1.when no value ls reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 09/16/9710:41
Sample 12483 FY 1997 Project: 97--0329
METALS SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JB007SL
Media: SOIL
RESULTS
17000J
0.61UJ
1.9J
88J
0.83JN
5.2JN
1200J
43J
13J
27J
24000J
1000JN
3200J
650J
0.13UJ
25J
3100J
0.33U
2.9J
70
0.38UJ
54J
110J
21
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
MD Number: MP76
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
SAS Number:TCLP .
lnorg Contractor: ANTEC
A-average value. NA-not analyzed. NAJ-interferences., J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 20:30
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 09/16/97 10:41
Sample 12483 FY 1997 Project: 97-0329
METALS TCLP SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB00?SL MD Number: MP76
Media: SOIL
RESULTS
0.008UJ
0.08J
1.23J
NA
0.008J
0.019J
NA
4.8J
NA
0.008J
NA
0.0002U
UNITS
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
TOTAL MERCURY
SAS Number:TCLP
lnorg Contractor: ANTEC
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 20:30
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 09/16/97 10:41
Sample 12484 FY 1997
METALS TCLP SCAN
Project: 97-0329
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF SAS Number:TCLP
ld/Station:JB008SL MD Number: MP77 lnorg Contractor: ANTEC
Media: SOIL
RESULTS
0.012J
0.018J
1.35J
NA
0.006J
0.011J
NA
0.19J
NA
0.005UJ
NA
0.0002U
UNITS
MG/L
MG/L
MG/L
MG/L·
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
TOTAL MERCURY
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 20:35
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound ITlay or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 09/16/97 10:41
Sample 12484 FY 1997
METALS SCAN
Project: 97-0329
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JB008SL
Media: SOIL
RESULTS
13000J
0.64UJ
0.53UR
130J
1JN
4.SJN
710J
27J
14J
27J
21000J
68JN
4100J
1000J
0.14UJ
23J
4800J
0.34U
4.2J
76
0.39UJ
45J
77J
28
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
MD Number: MP77
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 20:35
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value giVen. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA PRINTED 09/16/97 10:41
Sample 12485 FY 1997
METALS TCLP SCAN
Project: 97-0329
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC.
Program: NSF
ld/Station:JB009SL
Media: SOIL
RESULTS
0.009UJ
0.011J
1.6J
NA
0.007J
0.01U
NA
0.56J
NA
0.01J
NA
0.0002U
UNITS
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MGIL
MG/L
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
MD Number: MP78
TOTAL MERCURY
SAS Number:TCLP
lnorg Contractor: ANTEC
·A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 21 :45
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
METALS SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA PRINTED 09/16/97 10:41.
Sample 12485 FY 1997
METALS SCAN
Project: 97 -0329
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
ld/Station:JB009SL
Media: SOIL
RESULTS
7500J
1 UJ
1 UJ
87J
0.54J
2.7JN
960J
16J
9.6J
20J
12000J
49JN
2600J
710J
0.07UJ
15J
2800J
0.31U
1.7J
58
0.35U
26J
71J
8
UNITS
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
%
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
MD Number: MP78
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
% MOISTURE
SAS Number:TCLP
lnorg Contractor: ANTEC
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Printed by: Ron Phelps
Collected By:
Beginning: 08/13/97 21 :45
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
• •
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
MEMORANDUM
Date: 10/15/97
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of VOLATILES ORGANIC Sample Analysis
97-0328 JOHNSON CONTROLS GLOBE
WINSTON-SALEM, NC
From: John Mcconney r\,l~
To: PAT DEROSA
Thru: QA Office
•.
RECEIVED
OCT 16 1997
SUPERFUND SECTION
Attached are the results of analysis of samples collected as part of the subject project. If you have any
-questions, please contact me.
ATTACHMENT
• •
ORGANIC DATA QUALIFIER REPORT
Case Number 25633 Project Number 97-0328 SAS Number
NC Site ID. Johnson Controls Globe, Winston-salem,
Flag
Affected Samples Compound or Fraction Used
Volatiles
12413,12414,
12446,12448,
12450,12452,
12469,12473
12442
Extractables
12413, 12414,
12453,12455,
12458,12463,
12465,12466
12419
12424
12428
12445
12450
12467
12468
12469
toluene
trichloroethene
all compounds
4-chloro-3-methylphenol
4-nitrophenol
2,4-dinitrotoluene
pyrene
4-methylphenol
fluoranthene
pyrene
chrysene
benzo(b/K)fluoranthene
phenanthrene
carbazole
benzo(a)anthracene
benzo(b/k)fluoranthene
benzo(a)pyrene
indeno(l,2,3-cd)pyrene
benzo(g,h,i)perylene
acenaphthene
fluorene
anthracene
carbazole
dibenzo(a,h)anthracene
fluoranthene
pyrene
benzo(b/k)fluoranthene
phenanthrene
carbazole
dibenzo(a,h)anthracene
acenaphthene
dibenzofuran
fluorene
anthracene
fluoranthene
pyrene
chrysene
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
Reason
< quantitation limit
< quantitation limit
exceeded holding times
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitat .ton limit
< guantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitat:.on limit
< quantitat1.on limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
• •
ORGANIC DATA QUALIFIER REPORT
Case Number 25633
Affected Samples Compound or Fraction
Flag
Used Reason
13655
Pesticides
N/A
fluoranthene J
pyrene J
di-n-octylphthalate J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno{l,2,3-cd)pyrene J
dibenz(a,h)anthracene J
benzo(g,h,i)perylene J
< quantitation 1 irni t
< quantitation limit
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
recovery
recovery
recovery
recovery
recovery
recovery
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12462 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC001 SL
Media: SOIL D Number: MP70 Org Contractor: COMPU
RESULTS
11 U
11U
11U
11 U
11 U
11U
40U
11U
11U
11U
11U
11U
11U
11U
11 U
11 U
11U
11 U
11 U
11 U
11U
11U
11U
11U
11U
11U
11U
11U
11U
11U
11U
11 U
11 U
11
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENE$
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:15
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12463 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC101 SL
Media: SOIL
RESULTS UNITS
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
12 %
D Number: MP71
ANALYTE
CHLOROMETHANE
BROM OM ETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:15
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA
Sample 12463 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC 101 SL
Media: SOIL
RESULTS UNITS
6JN UG/KG
D Number: MP71
ANALYTE
DIMETHYL SULFIDE
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:15
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12464 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC003SL
Media: SOIL
RESULTS
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
25
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MP72
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 18:30
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12465 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC004SL
Media: SOIL
RES UL TS UNITS
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
39 %
Case Number: 25633
D Number: MP73
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:45
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12466 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC005SL
Media: SOIL
RESULTS UNITS
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11 U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11 %
D Number: MP74
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAJ-interierences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:00
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-materiat was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12467 FY 1997
VOLATILES SCAN
Project: 97 -0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC006SL
Media: SOIL
RESULTS
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
16U
36
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MP75
ANALYTE
CHLOROMETHANE
BROM OM ETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COM PU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:00
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12468 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC007SL
Media: SOIL
RESULTS
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
20
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MP76
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:30
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12469 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC00BSL
Media: SOIL
RESULTS UNITS
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
2J UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
7 %
Case Number: 25633
D Number: MP77
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROM OF ORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:35
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-materlal was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12470 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC009SL
Media: SOIL
RESULTS UNITS
11U UG/KG
11U UG/KG
11 U UG/KG
11U UG/KG
11 U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11 U UG/KG
11U UG/KG
11U UG/KG
9 %
Case Number: 25633
D Number: MP78
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 21:45
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 13655 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC010SL
Media: SOIL
RESULTS
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
21
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MP65
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:20
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12455 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC011 SL MD Number: MP66 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SOIL
RESULTS UNITS
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
23 %
D Number: MP66
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1,1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 16:25
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12456 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC012SL
Media: SOIL
RESULTS
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
28
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
Case Number: 25633
MD Number: MP67
D Number: MP67
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:56
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12444 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC013SL MD Number: MP54 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SOIL
RESULTS
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
21
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MP54
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08113/97 11 :50
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12445 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC014SL MD Number: MP55 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SOIL
RESULTS
12U
12U
12U
12U
12U
12U
20U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
17
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MP55
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/9715:45
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12442 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC001 SW
Media: SURFACEWA
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
9J UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
Case Number: 25633
MD Number: MP52
D Number: MP52
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :00
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12443 FY 1997 Project: 97 -0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC001 SD MD Number: MP53 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
41
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MP53
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAJ-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :30
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. Li-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12447 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC002SW
Media: SURFACEWA
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UG/L
10U UGIL
10U UGIL
Case Number: 25633
MD Number: MP57
D Number: MP57
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROM OF ORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:45
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12446 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC002SD
Media: SEDIM
RES UL TS UNITS
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
2J UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
35 %
Case Number: 25633
MD Number: MP56
D Number: MP56
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 12:30
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantftation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12448 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC003SD MD Number: MP58 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS UNITS
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
30U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
2J UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
31 %
D Number: MP58
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11:15
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12449 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC004SW
Media: SURFACEWA
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
Case Number: 25633
MD Number: MP59
D Number: MP59
CH LOR OM ETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COM PU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROM OF ORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 10:05
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12450 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC004SD MD Number: MP60 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
17U
2J
17U
17U
17U
17U
41
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MP60
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1,1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROM OF ORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08113197 10:30
Ending:
K-actual value ls known to be less than value given. L-actual value is known to be greater than value given. Li-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12451 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC005SW MD Number: MP61 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA D Number: MP61
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 12:05
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12452 FY 1997 Project: 97 -0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC005SD
Media: SEDIM
RESULTS
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
2J
15U
15U
15U
35
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
Case Number: 25633
MD Number: MP62
D Number: MP62
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
I norg Contractor: CH EM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 12:35
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA
Sample 12422 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC006SW
Media: SURFACEWA
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
Case Number: 25633
MD Number: MH94
D Number: MH94
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYLISOBUTYLKETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 12:25
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12423 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC 106SW
Media: SURFACEWA
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
Case Number: 25633
MD Number: MH95
D Number: MH95
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 12:30
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12424 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC006SD
Media: SEDIM
RESULTS
42U
42U
42U
42U
42U
42U
270U
42U
42U
89
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
42U
76
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
Case Number: 25633
MD Number: MH96
D Number: MH96
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 13:00
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12434 FY 1997
VOLATILES SCAN
Project: 97 -0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC007SW
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
Case Number: 25633
MD Number: MK09
D Number: MK09
CHLO ROM ETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAJ-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:26
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA
Sample 12436 FY 1997 Project: 97 -0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC107SW MD Number: MK11 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA D Number: MK11
RESULTS
10U
10U
10U
10U
10U
10U
40U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:26
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12435 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC007SD MD Number: MK10 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS
30U
30U
30U
30U
30U
30U
100U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
30U
67
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MK10
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:55
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampting and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12438 FY 1997
VOLATILES SCAN
Project: 97 -0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC00SSW
Media: SURFACEWA
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
Case Number: 25633
MD Number: MK13
D Number: MK13
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 19:25
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12437 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC008SD MD Number: MK12 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS UNITS
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
30U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
34 %
D Number: MK12
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA
Sample 12439 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC 108SD
Media: SEDIM
RESULTS UNITS
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
40U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
33 %
Case Number: 25633
MD Number: MK14
D Number: MK14
ANALYTE
CHLOROMETHANE
BROM OM ETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
e
•
VOLATILES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12441 FY 1997 Project: 97 -0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC009SW MD Number: MP51 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA D Number: MP51
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:45
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12440 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC009SD
Media: SEDIM
RESULTS UNITS
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
ZOU UG/KG
60U UG/KG
ZOU UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
ZOU UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
ZOU UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
ZOU UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
51 %
Case Number: 25633
MD Number: MP50
D Number: MP50
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interterences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:30
Ending:
K-actual value is known to be less than value given. L-actual value ls known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems; 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12453 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC010SW MD Number: MP63 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA D Number: MP63
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 09:40
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12454 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC010SD
Media: SEDIM
RESULTS
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
24
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
-UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
Case Number: 25633
MD Number: MP64
D Number: MP64
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 09:25
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12429 FY 1997
VOLATILES SCAN
Project: 97 -0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC011 SW
Media: SURFACEWA
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
Case Number: 25633
MD Number: MJ01
D Number: MJ01
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:25
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12430 FY 1997 Project: 97 -0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC011 SD
Media: SEDIM
RESULTS
15U
15U
15U
15U
15U
15U
40U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
15U
34
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
Case Number: 25633
MD Number: MJ02
D Number: MJ02
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12420 FY 1997 Project: 97 -0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC012SW
Media: SURFACEWA ·
Case Number: 25633
MD Number: MH92
D Number: MH92
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1,1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROM OF ORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 11 :12
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12421 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC012SD
Media: SEDIM
RESULTS UNITS
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
SOU UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
15U UG/KG
33 %
Case Number: 25633
MD Number: MH93
D Number: MH93
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1,1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 11 :30
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12431 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC013SW
Media: SURFACEWA
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UGIL
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UG/L
10U UG/L
10U UG/L
Case Number: 25633
MO Number: MK06
D Number: MK06
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08112/97 16:35
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12432 FY 1997
VOLATILES SCAN
Project: 97 -0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC013SD
Media: SEDIM
RESULTS UNITS
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
27 %
Case Number: 25633
MD Number: MK07
D Number: MK07
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:50
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12419 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC014SW MD Number: MH91 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA D Number: MH91
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:45
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12418 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC014SD MD Number: MH90 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS
23U
23U
23U
23U
23U
23U
30U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
23U
56
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MH90
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1,1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1 ,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROM OF ORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:33
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12427 FY 1997 Project: 97 -0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC015SW MD Number: MH99 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SURFACEWA D Number: MH99
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1,1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 11 :47
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12428 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC015SD
Media: SEDIM
RESULTS
18U
18U
18U
18U
18U
18U
40U
18U
18U
18U
18U
18U
18U
18U
18U
18U
18U
18U
18U
18U
18U
18U
18U
18U
18U
18U
18U
18U
18U
18U
18U
18U
18U
45
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
Case Number: 25633
MD Number: MJ00
D Number: MJ00
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/9712:15
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resamp!ing and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12433 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC016SD MD Number: MK0B lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS UNITS
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
32U UG/KG
69 %
D Number: MK0B
ANALYTE
CH LOR OM ETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1,1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John McConney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 15:35
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12425 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC017SW
Media: SURFACEWA
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
Case Number: 25633
MD Number: MH97
D Number: MH97
CHLO ROM ETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:30
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12426 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC017SD MD Number: MH98 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
20
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MH98
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROM OF ORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:40
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12412 FY 1997
VOLATILES SCAN
Project: 97 -0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC018SW
Media: SURFACEWA
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
Case Number: 25633
MD Number: LL02
D Number: LL02
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 16:32
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12413 FY 1997 Project: 97 -0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC018SD
Media: SEDIM
RESULTS UNITS
28U UGIKG
28U UGIKG
28U UGIKG
28U UGIKG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
4J UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
28U UG/KG
64 %
Case Number: 25633
MD Number: LL03
D Number: LL03
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1,1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08111197 17:35
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12414 FY 1997
VOLATILES SCAN
Project: 97 -0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC019SD MD Number: LL04 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS UNITS
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
4J UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
58 %
D Number: LL04
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLO RO ETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 17:50
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-materiat was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12415 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC020SW
Media: SURFACEWA
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
Case Number: 25633
MD Number: LL05
D Number: LL05
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11 /97 15:00
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12416 FY 1997
VOLATILES SCAN
Project: 97 -0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC021 SW MD Number: LL06
Media: SURFACEWA D Number: LL06
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
10U UG/L
10U UG/L
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 17:00
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12417 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC021 SD MD Number: MH89 lnorg Contractor: CHEM
Org Contractor: COMPU Media: SEDIM
RESULTS
24U
24U
24U
24U
30U
24U
140U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
59
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MH89
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 18:40
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12457 FY 1997
VOLATILES SCAN
Project: 97-0328
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC001 PW MD Number: MP68 lnorg Contractor: CHEM
Org Contractor: COMPU Media: GROUNDWA
RES UL TS UNITS
10U UGIL
10U UGIL
10U UGIL
10U UGIL
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
D Number: MP68
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08113197 20:15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12458 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC002PW
Media: GROUNDWA
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
Case Number: 25633
MD Number: MP69
D Number: MP69
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTALXYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 21 :00
Ending:
K-actual value is known to be fess than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12471 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC001TB
Media: WATER
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: MP79
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11 /97 13:45
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-rnaterial was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12472 FY 1997 Project: 97-0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC002TB
Media: WATER
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
Case Number: 25633
D Number: MPS0
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 13:45
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
VOLATILES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12473 FY 1997 Project: 97 -0328
VOLATILES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC003TB
Media: SOIIL
RESULTS UNITS
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
40U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
2J UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
4 %
Case Number: 25633
D Number: MP81
ANALYTE
CHLO ROM ETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
Org Contractor: COMPU
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 08:25
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 07:30
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
MEMORANDUM
Date: 10/15/97
• •
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of EXTRACTABLES ORGANIC Sample Analysis
97-0328 JOHNSON CONTROLS GLOBE
WINSTON-SALEM, NC
From: John Mcconney
To: PAT DEROSA
RECEIVED
OCT 16 1997
SUPERFUND SECTION
Thru: QA Office
Attached are the results of analysis of samples collected as part of the subject project. If you have any
questions, please contact me.
I
ATTACHMENT
\
• •
ORGANIC DATA QUALIFIER REPORT
Case Number 25633 Project Number 97-0328 SAS Number
NC Site ID. Johnson Controls Globe, Winston-salem,
Affected Samples
Volatiles
12413, 12414,
12446,12448,
12450,12452,
12469,12473
12442
Extractables
12413, 12414,
12453,12455,
12458,12463,
12465,12466
12419
12424
12428
12445
12450
12467
12468
12469
Compound or Fraction
toluene
trichloroethene
all compounds
4-chloro-3-methylphenol
4-nitrophenol
2,4-dinitrotoluene
pyrene
4-methylphenol
fluoranthene
pyrene
chrysene
benzo(b/K)fluoranthene
phenanthrene
carbazole
benzo(a)anthracene
benzo(b/k)fluoranthene
benzo(a)pyrene.
indeno(l,2,3-cd)pyrene
benzo(g,h,i)perylene
acenaphthene
fluorene
anthracene
carbazole
dibenzo(a,h)anthracene
fluoranthene
pyrene
benzo(b/k)fluoranthene
phenanthrene
carbazole
dibenzo(a,h)anthracene
acenaphthene
dibenzofuran
fluorene
anthracene
fluoranthene
pyrene
chrysene
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
Flag
Used Reason
< quantitation limit
< quantitation limit
exceeded holding times
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitatiol1 limit
< quantitation limit
< quantitation limit
< quantitation limit
< qu.3.ntitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitatlon limit
< quantitati.on limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
•
ORGANIC DATA QUALIFIER REPORT
Case Number 25633
Flag
Affected Samples Compound or Fraction Used
13655 fluoranthene J
Pesticides
N/A
pyrene J
di-n-octylphthalate J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
dibenz(a,h)anthracene J
benzo(g,h,i)perylene J
Reason
< quantitation limit
< quantitation limit
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
re'covery
recovery
recovery
recovery
recovery
recovery
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12462 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC001 SL
Media: SOIL
RESULTS
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
930U
370U
370U
370U
370U
370U
370U
930U
370U
930U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
Case Number: 25633
D Number: MP70
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
Org Contractor: COMPU
RESULTS
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
930U
370U
930U
930U
930U
930U
370U
11
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/9717:15
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
OI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12462 FY 1997 Project: 97 -0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC001 SL
Media: SOIL
RESULTS UNITS
400J UGIKG
Case Number: 25633
D Number: MP70 Org Contractor: COMPU
ANALYTE
1 UNIDENTIFIED COMPOUND
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08113197 17:15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12463 FY 1997 Project: 97-0328
EXTRACT ABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC101SL
Media: SOIL
RESULTS
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
940UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
940UJ
370UJ
940UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
Case Number: 25633
D Number: MP71
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
EXCESSIVE HOLDING TIME
Org Contractor: COMPU
RESULTS
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
940UJ
370UJ
940UJ
940UJ
940UJ
940UJ
370UJ
12
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:15
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems; 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12463 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC101 SL
Media: SOIL
RESULTS UNITS
1 0000J UG/KG
5000J UG/KG
Case Number: 25633
D Number: MP71
ANALYTE
7 UNIDENTIFIED COMPOUNDS
ALKANES
Org Contractor: COM PU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:15
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12464 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC003SL
Media: SOIL
RESULTS UNITS
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
1100U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
1100U UG/KG
440U UG/KG
1100U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
Case Number: 25633
D Number: MP72
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE (HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
Org Contractor: COMPU
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 18:30
Ending:
RES UL TS UNITS ANALYTE
440U UG/KG BIS(2-ETHYLHEXYL) PHTHALATE
440U UG/KG BENZO(A)ANTHRACENE
440U UG/KG CHRYSENE
440U UG/KG 3,3'-DICHLOROBENZIDINE
440U UG/KG DI-N-OCTYLPHTHALATE
440U UG/KG BENZO(B AND/OR K)FLUORANTHENE
440U UG/KG BENZO-A-PYRENE
440U UG/KG INDENO (1,2,3-CD) PYRENE
440U UG/KG DIBENZO(A,H)ANTHRACENE
440U UG/KG BENZO(GHl)PERYLENE
440U UG/KG 2-CHLOROPHENOL
440U UG/KG 2-METHYLPHENOL
440U UG/KG (3-AND/OR 4-)METHYLPHENOL
440U UG/KG 2-NITROPHENOL
440U UG/KG PHENOL
440U UG/KG 2,4-DIMETHYLPHENOL
440U UG/KG 2,4-DICHLOROPHENOL
440U UG/KG 2,4,6-TRICHLOROPHENOL
1100U UG/KG 2,4,5-TRICHLOROPHENOL
440U UG/KG 4-CHLORO-3-METHYLPHENOL
1100U UG/KG 2,4-DINITROPHENOL
1100U UG/KG 2-METHYL-4,6-DINITROPHENOL
1100U UG/KG PENTACHLOROPHENOL
1100U UG/KG 4-NITROPHENOL
440U UG/KG CARBAZOLE
25 % % MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12465 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC004SL
Media: SOIL
RES UL TS UNITS
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
1400UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
1400UJ UG/KG
540UJ UG/KG
1400UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
540UJ UG/KG
160J UG/KG
130J UG/KG
540UJ UG/KG
D Number: MP73
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
EXCESSIVE HOLDING TIME
Org Contractor: COMPU
RESULTS
540UJ
68J
190J
540UJ
540UJ
280J
74J
540UJ
540UJ
540UJ
540UJ
540UJ
540UJ
540UJ
540UJ
540UJ
540UJ
540UJ
1400UJ
540UJ
1400UJ
1400UJ
1400UJ
1400UJ
540UJ
39
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:45
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12465 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC004SL
Media: SOIL
RES UL TS UNITS
100JN UG/KG
600J UG/KG
Case Number: 25633
D Number: MP73
ANALYTE
BENZOPYRENE (NOT A)
1 UNIDENTIFIED COMPOUND
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:45
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12466 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC005SL
Media: SOIL
RESULTS
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
930UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
930UJ
370UJ
930UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
Case Number: 25633
D Number: MP74
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
EXCESSIVE HOLDING TIME
Org Contractor: COMPU
RESULTS
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
370UJ
930UJ
370UJ
930UJ
930UJ
930UJ
930UJ
370UJ
11
A-average value. NA-not analyzed. NAl-interferences. J-estimated vatue. N-presumptrve evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:00
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
e
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12466 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC005SL
Media: SOIL
RESULTS UNITS
1000J UG/KG
Case Number: 25633
D Number: MP74 Org Contractor: COMPU
ANALYTE
1 UNIDENTIFIED COMPOUND
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:00
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12467 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC006SL
Media: SOIL
RESULTS UNITS
510U
510U
510U
510U
510U
510U
510U
510U
510U
510U
510U
510U
510U
510U
510U
510U
510U
1300U
510U
510U
510U
510U
510U
510U
1300U
510U
1300U
510U
510U
510U
510U
510U
460J
510U
510U
1800
1400
510U
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
Case Number: 25633
D Number: MP75
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
Org Contractor: COMPU
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:00
Ending:
RESULTS UNITS ANALYTE
510U
610
1300
510U
510U
2800
1000
810
220J
870
510U
510U
510U
510U
510U
510U
510U
510U
1300U
510U
1300U
1300U
1300U
1300U
95J
36
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12467 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC006SL
Media: SOIL
RESULTS
300JN
200JN
300JN
100JN
100JN
100JN
1000JN
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
Case Number: 25633
D Number: MP75
ANALYTE
ANTHRACENEDIONE
BENZOFLUORENE
BENZANTHRACENONE (2 ISOMERS)
BENZONAPHTHOTHIOPHENE
NAPHTHACENEDIONE
BENZOFLUORANTHENE (NOT B OR K)
BENZOPYRENE (NOT A, 2 ISOMERS)
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:00
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12468 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC007SL
Media: SOIL D Number: MP76
RESULTS UNITS ANALYTE
410U UG/KG 1,3-DICHLOROBENZENE
410U UG/KG 1,4-DICHLOROBENZENE
410U UG/KG 1,2-DICHLOROBENZENE
410U UG/KG BIS(2-CHLOROETHYL) ETHER
410U UG/KG HEXACHLOROETHANE
410U UG/KG BIS(2-CHLOROISOPROPYL) ETHER
410U UG/KG N-NITROSODI-N-PROPYLAMINE
410U UG/KG NITROBENZENE
410U UG/KG HEXACHLOROBUTADIENE
410U UG/KG 2-METHYLNAPHTHALENE
410U UG/KG 1,2,4-TRICHLOROBENZENE
410U UG/KG NAPHTHALENE
410U UG/KG 4-CHLOROANILINE
410U UG/KG BIS(2-CHLOROETHOXY)METHANE
410U UG/KG ISOPHORONE
410U UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP)
410U UG/KG 2-CHLORONAPHTHALENE
1000U UG/KG 2-NITROANILINE
410U UG/KG ACENAPHTHYLENE
64J UG/KG ACENAPHTHENE
410U UG/KG DIMETHYL PHTHALATE
47J UG/KG DIBENZOFURAN
410U UG/KG 2,4-DINITROTOLUENE
410U UG/KG 2,6-DINITROTOLUENE
1000U UG/KG 3-NITROANILINE
410U UG/KG 4-CHLOROPHENYL PHENYL ETHER
1000U UG/KG 4-NITROANILINE
100J UG/KG FLUORENE
410U UG/KG DIETHYL PHTHALATE
410U UG/KG N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
410U UG/KG HEXACHLOROBENZENE(HCB)
410U UG/KG 4-BROMOPHENYL PHENYL ETHER
3200 UG/KG PHENANTHRENE
200J UG/KG ANTHRACENE
410U UG/KG D1-N-BUTYLPHTHALATE
7600 UG/KG FLUORANTHENE
5900 UG/KG PYRENE
410U UG/KG BENZYLBUTYLPHTHALATE
Org Contractor: COMPU
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:30
Ending:
RES UL TS UNITS ANALYTE
410U UG/KG BIS(2-ETHYLHEXYL) PHTHALATE
2300 UG/KG BENZO(A)ANTHRACENE
4300 UG/KG CHRYSENE
410U UG/KG 3,3'-DICHLOROBENZIDINE
410U UG/KG DI-N-OCTYLPHTHALATE
8000 UG/KG BENZO(B AND/OR K)FLUORANTHENE
3600 UG/KG BENZO-A-PYRENE
2900 UG/KG INDENO (1,2,3-CD) PYRENE
760 UG/KG DIBENZO(A,H)ANTHRACENE
3100 UG/KG BENZO(GHl)PERYLENE
410U UG/KG 2-CHLOROPHENOL
410U UG/KG 2-METHYLPHENOL.
410U UG/KG (3-AND/OR 4-)METHYLPHENOL
410U UG/KG 2-NITROPHENOL
410U UG/KG PHENOL
410U UG/KG 2,4-DIMETHYLPHENOL
410U UG/KG 2,4-DICHLOROPHENOL
410U UG/KG 2,4,6-TRICHLOROPHENOL
1000U UG/KG 2,4,5-TRICHLOROPHENOL
410U UG/KG 4-CHLORO-3-METHYLPHENOL
1000U UG/KG 2,4-DINITROPHENOL
1000U UG/KG 2-METHYL-4,6-DINITROPHENOL
1000U UG/KG PENTACHLOROPHENOL
1000U UG/KG 4-NITROPHENOL
690 UG/KG CARBAZOLE
20 % % MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resarnpling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12468 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC007SL
Media: SOIL
RESULTS
300JN
700JN
800JN
200JN
2000JN
300JN
300JN
90JN
300JN
300JN
200JN
7000JN
8000J
200JN
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
ACRIDINE
Case Number: 25633
D Number: MP76
METHYLANTHRACENE (2 ISOMERS)
CYCLOPENTAPHENANTHRENE
PHENYLNAPHTHALENE
ANTHRACENEDIONE
NAPHTHALIC ANHYDRIDE
CYCLOPENTAPHENANTHRENONE
METHYLPYRENE
BENZOFLUORENE (2 ISOMERS)
BENZANTHRACENONE (2 ISOMERS)
BENZONAPHTHOTHIOPHENE
BENZOPYRENE (NOT A, 3 ISOMERS)
4 UNIDENTIFIED COMPOUNDS
NAPHTHCENEDIONE
Org Contractor: COMPU
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12469 FY 1997 Project: 97 -0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC00SSL
Media: SOIL
RES UL TS UNITS
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
890U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
890U UG/KG
350U UG/KG
890U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
54J UG/KG
50J UG/KG
350U UG/KG
Case Number: 25633
D Number: MP77
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITRO BENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:35
Ending:
Org Contractor: COMPU
RESULTS UNITS
350U UG/KG
350U UG/KG
42J UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
890U UG/KG
350U UG/KG
890U UG/KG
890U UG/KG
890U UG/KG
890U UG/KG
350U UG/KG
7 %
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-N ITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA
Sample 12469 FY 1997 Project: 97 -0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC008SL
Media: SOIL
RES UL TS UNITS ANAL YTE
Case Number: 25633
D Number: MP77
400JN UG/KG NAPTHOCHRYSENE (2 ISOMERS)
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:35
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
e
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12470 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC009SL
Media: SOIL D Number: MP78 Org Contractor: COMPU
RESULTS UNITS ANALYTE RESULTS
360U UG/KG 1,3-DICHLOROBENZENE 360U
360U UG/KG 1,4-DICHLOROBENZENE 360U
360U UG/KG 1,2-DICHLOROBENZENE 360U
360U UG/KG BIS(2-CHLOROETHYL) ETHER 360U
360U UG/KG HEXACHLOROETHANE 360U
360U UG/KG BIS(2-CHLOROISOPROPYL) ETHER 360U
360U UG/KG N-NITROSODI-N-PROPYLAMINE 360U
360U UG/KG NITROBENZENE 360U
360U UG/KG HEXACHLOROBUTADIENE 360U
360U UG/KG 2-METHYLNAPHTHALENE 360U
360U UG/KG 1,2,4-TRICHLOROBENZENE 360U
360U UG/KG NAPHTHALENE 360U
360U UG/KG 4-CHLOROANILINE 360U
360U UG/KG BIS(2-CHLOROETHOXY)METHANE 360U
360U UG/KG ISOPHORONE 360U
360U UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP) 360U
360U UG/KG 2-CHLORONAPHTHALENE 360U
910U UG/KG 2-NITROANILINE 360U
360U UG/KG ACENAPHTHYLENE 910U
360U UG/KG ACENAPHTHENE 360U
360U UG/KG DIMETHYL PHTHALATE 910U
360U UG/KG DIBENZOFURAN 910U
360U UG/KG 2,4-DINITROTOLUENE 910U
360U UG/KG 2,6-DINITROTOLUENE 910U
910U UG/KG 3-NITROANILINE 360U
360U UG/KG 4-CHLOROPHENYL PHENYL ETHER 9
910U UG/KG 4-NITROANILINE
360U UG/KG FLUORENE
360U UG/KG DIETHYL PHTHALATE
360U UG/KG N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
360U UG/KG HEXACHLOROBENZENE(HCB)
360U UG/KG 4-BROMOPHENYL PHENYL ETHER
360U UG/KG PHENANTHRENE
360U UG/KG ANTHRACENE
360U UG/KG DI-N-BUTYLPHTHALATE
360U UG/KG FLUORANTHENE
360U UG/KG PYRENE
360U UG/KG BENZYL BUTYL PHTHALATE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 21 :45
Ending:
UNITS ANALYTE
UG/KG BIS(2-ETHYLHEXYL) PHTHALATE
UG/KG BENZO(A)ANTHRACENE
UG/KG CHRYSENE
UG/KG 3,3'-DICHLOROBENZIDINE
UG/KG DI-N-OCTYLPHTHALATE
UG/KG BENZO(B AND/OR K)FLUORANTHENE
UG/KG BENZO-A-PYRENE
UG/KG INDENO (1,2,3-CD) PYRENE
UG/KG DIBENZO(A,H)ANTHRACENE
UG/KG BENZO(GHl)PERYLENE
UG/KG 2-CHLOROPHENOL
UG/KG 2-METHYLPHENOL
UG/KG (3-AND/OR 4-)METHYLPHENOL
UG/KG 2-NITROPHENOL
UG/KG PHENOL
UG/KG 2,4-DIMETHYLPHENOL
UG/KG 2,4-DICHLOROPHENOL
UG/KG 2,4,6-TRICHLOROPHENOL
UG/KG 2,4,5-TRICHLOROPHENOL
UG/KG 4-CHLORO-3-METHYLPHENOL
UG/KG 2,4-DINITROPHENOL
UG/KG 2-METHYL-4,6-DINITROPHENOL
UG/KG PENTACHLOROPHENOL
UG/KG 4-NITROPHENOL
UG/KG CARBAZOLE
% % MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resamp1ing and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 13655 FY 1997 Project: 97 -0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC01 0SL
Media: SOIL
RESULTS
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
1000U
420U
420U
420U
420U
420U
420U
1000U
420U
1000U
420U
420U
420U
420U
420U
420U
420U
420U
54J
45J
420U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MP65
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
Org Contractor: COMPU
RESULTS
420U
420U
420U
420U
420UJ
420UJ
420UJ
420UJ
420UJ
420UJ
420U
420U
420U
420U
420U
420U
420U
420U
1000U
420U
1000U
1000U
1000U
1000U
420U
21
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:20
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limlt.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems; 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 13655 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC01 0SL
Media: SOIL
RESULTS UNITS
2000J UG/KG
Case Number: 25633
D Number: MP65 Org Contractor: COMPU
ANALYTE
3 UNIDENTIFIED COMPOUNDS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08113/97 17:20
Ending:
K-actual value is known to be Jess than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12455 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC011 SL
Media: SOIL
RES UL TS UNITS
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
1100UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
1100UJ
430UJ
1100UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MP66
D Number: MP66
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE (HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
EXCESSIVE HOLDING TIME
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
430UJ
1100UJ
430UJ
1100UJ
1100UJ
1100UJ
11 OOUJ
430UJ
23
A-average value. NA-not analyzed. NAl-interierences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 16:25
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALA TE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12456 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC012SL MD Number: MP67
Media: SOIL
RES UL TS UNITS
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
1100U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
1100U UG/KG
460U UG/KG
1100U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
460U UG/KG
D Number: MP67
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITRO BENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
460U
1100U
460U
1100U
1100U
1100U
1100U
460U
28
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John McConney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 17:56
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
K-actual value is known to be Jess than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12456 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC012SL
Media: SOIL
RES UL TS UNITS ANAL YTE
Case Number: 25633
MD Number: MP67
D Number: MP67
500J UGIKG 1 UNIDENTIFIED COMPOUND
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-eslimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08113197 17:56
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12444 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC013SL MD Number: MP54
Media: SOIL
RESULTS
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
1000U
420U
420U
420U
420U
420U
420U
1000U
420U
1000U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MP54
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
420U
1000U
420U
1000U
1000U
1000U
1000U
420U
21
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :50
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12444 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC013SL
Media: SOIL
RES UL TS UNITS
400JN UG/KG
1000J UG/KG
Case Number: 25633
MD Number: MP54
D Number: MP54
ANALYTE
CARBOXYLIC ACID
2 UNIDENTIFIED COMPOUNDS
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :50
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12445 FY 1997 Project: 97-0328
EXTRACTABLE$ SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC014SL
Media: SOIL
RESULTS
400U
400U
400U
400U
400U
400U
400U
400U
400U
400U
400U
400U
400U
400U
400U
400U
400U
1000U
400U
44J
400U
400U
400U
400U
1000U
400U
1000U
65J
400U
400U
400U
400U
1700
110J
400U
5400
2900
400U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MP55
D Number: MP55
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
400U
1200
2300
400U
400U
4300
1800
940
270J
860
400U
400U
400U
400U
400U
400U
400U
400U
1000U
400U
1000U
1000U
1000U
1000U
390J
17
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 15:45
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12445 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC014SL
Media: SOIL
RESULTS
90JN
500JN
700JN
100JN
100JN
100JN
300JN
100JN
200JN
2000JN
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
ACRIDINE
Case Number: 25633
MD Number: MP55
D Number: MP55
METHYLANTHRACENE (3 ISOMERS)
ANTHRACENEDIONE
NAPHTHALIC ANHYDRIDE
CYCLOPENTAPHENANTHRENONE
BENZOFLUORENE
BENZANTHRACENONE (3 ISOMERS)
BENZONAPHTHOTHIOPHENE
BENZOFLUORANTHENE (NOT B OR K)
BENZOPYRENE (NOT A, 2 ISOMERS)
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 15:45
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA. Production Date: 10/15/97 09:00
Sample 12442 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC001 SW MD Number: MP52
Media: SURFACEWA D Number: MP52
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
I norg Contractor: CH EM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :00
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALA TE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12443 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC001 SD MD Number: MP53
Media: SEDIM
RESULTS
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
1400U
560U
560U
560U
560U
560U
560U
1400U
560U
1400U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MP53
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
560U
1400U
560U
1400U
1400U
1400U
1400U
560U
41
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :30
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12443 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC001 SD
Media: SEDIM
RESULTS
1000JN
200JN
3000J
UNITS
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MP53
D Number: MP53
PINENE (2 ISOMERS)
DIMETHOXYPROPENYLPHENOL
3 UNIDENTIFIED COMPOUNDS
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAJ-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John McConney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :30
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12447 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC002SW MD Number: MP57
Media: SURFACEWA
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
D Number: MP57
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
D1-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 19:45
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value ls reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12446 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC002SD
Media: SEDIM
RESULTS
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
1300U
500U
500U
500U
500U
500U
500U
1300U
500U
1300U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MP56
D Number: MP56
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
1300U
500U
1300U
1300U
1300U
1300U
500U
35
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 12:30
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R--qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACT ABLES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12446 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC002SD
Media: SEDIM
RESULTS UNITS
400JN UG/KG
Case Number: 25633
MD Number: MP56
D Number: MP56
ANALYTE
CARBOXYLIC ACID
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presurnptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13197 12:30
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12448 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC003SD MD Number: MP58
Media: SEDIM
RESULTS UNITS
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
1200U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
1200U UG/KG
470U UG/KG
1200U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
470U UG/KG
D Number: MP58
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
470U
1200U
470U
1200U
1200U
1200U
1200U
470U
31
A-average value. NA-not analyzed. NAl-interierences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11 :15
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12448 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC003SD
Media: SEDIM
RESULTS
300JN
1000J
UNITS
UG/KG
UG/KG
Case Number: 25633
MD Number: MP58
D Number: MP58
ANALYTE
CARBOXYLIC ACID
ALKANES
I norg Contractor: CH EM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 11: 15
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems; 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
G
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12449 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC004SW
Media: SURFACEWA
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UGIL
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UGIL
10U UG/L
10U UG/L
ANALYTE
Case Number: 25633
MD Number: MP59
D Number: MP59
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITRO BENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINEIDIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 10:05
Ending:
UNITS
UGIL
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UGIL
UGIL
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12450 FY 1997 Project: 97-0328
EXTRACT ABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC004SD
Media: SEDIM
RESULTS
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
1400U
550U
550U
550U
550U
550U
550U
1400U
550U
1400U
550U
550U
550U
550U
550U
550U
550U
550U
87J
63J
550U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MP60
D Number: MP60
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
I norg Contractor: CH EM
Org Contractor: COMPU
RESULTS
550U
550U
550U
550U
550U
87J
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
550U
1400U
550U
1400U
1400U
1400U
1400U
550U
41
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 10:30
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12450 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC004SD
Media: SEDIM
RESULTS UNITS
300JN UG/KG
3000J UG/KG
3000J UG/KG
Case Number: 25633
MD Number: MP60
D Number: MP60
ANALYTE
CARBOXYLIC ACID
ALKANES
2 UNIDENTIFIED COMPOUNDS
I norg Contractor: CH EM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 10:30
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12451 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC005SW
Media: SURFACEWA
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U -UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
Case Number: 25633
MD Number: MP61
D Number: MP61
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITRO BENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALA TE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 12:05
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3°AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACT ABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12452 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC005SD
Media: SEDIM
RESULTS
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
1200U
500U
500U
500U
500U
500U
500U
1200U
500U
1200U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MP62
D Number: MP62
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
1200U
500U
1200U
1200U
1200U
1200U
500U
35
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/9712:35
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12452 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC005SD
Media: SEDIM
RESULTS
600J
700J
UNITS
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MP62
D Number: MP62
1 UNIDENTIFIED COMPOUND
ALKANES
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 12:35
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampllng and reanalysis is necessary for verification.
C-confirmed by gems; 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12422 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC006SW
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
Case Number: 25633
MD Number: MH94
D Number: MH94
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 12:25
Ending:
lnorg Contractor: CHEM
Org Contractor: COMPU
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
25U UG/L
25U UG/L
25U UG/L
10U UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12423 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC 106SW
Media: SURFACEWA
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
Case Number: 25633
MD Number: MH95
D Number: MH95
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 12:30
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. Li-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12424 FY 1997 Project: 97-0328
EXTRACTABLE$ SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC006SD
Media: SEDIM
RESULTS UNITS
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
3400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
3400U UG/KG
1400U UG/KG
3400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
1400U UG/KG
230J UG/KG
160J UG/KG
1400U UG/KG
ANALYTE
Case Number: 25633
MD Number: MH96
D Number: MH96
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
1400U
1400U
180J
1400U
1400U
210J
1400U
1400U
1400U
1400U
1400U
1400U
150J
1400U
1400U
1400U
1400U
1400U
3400U
1400U
3400U
3400U
3400U
3400U
1400U
76
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 13:00
Ending:
UNITS ANALYTE
UG/KG BIS(2-ETHYLHEXYL) PHTHALATE
UG/KG BENZO(A)ANTHRACENE
UG/KG CHRYSENE
UG/KG 3,3'-DICHLOROBENZIDINE
UG/KG DI-N-OCTYLPHTHALA TE
UG/KG BENZO(B AND/OR K)FLUORANTHENE
UG/KG BENZO-A-PYRENE
UG/KG INDENO (1,2,3-CD) PYRENE
UG/KG DIBENZO(A,H)ANTHRACENE
UG/KG BENZO(GHl)PERYLENE
UG/KG 2-CHLOROPHENOL
UG/KG 2-METHYLPHENOL
UG/KG (3-AND/OR 4-)METHYLPHENOL
UG/KG 2-NITROPHENOL
UG/KG PHENOL
UG/KG 2,4-DIMETHYLPHENOL
UG/KG 2,4-DICHLOROPHENOL
UG/KG 2,4,6-TRICHLOROPHENOL
UG/KG 2,4,5-TRICHLOROPHENOL
UG/KG 4-CHLORO-3-METHYLPHENOL
UG/KG 2,4-DINITROPHENOL
UG/KG 2-METHYL-4,6-DINITROPHENOL
UG/KG PENTACHLOROPHENOL
UG/KG 4-NITROPHENOL
UG/KG CARBAZOLE
% % MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12424 FY 1997 Project: 97 -0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC006SD MD Number: MH96
Media: SEDIM
RESULTS
2000JN
3000J
UNITS
UG/KG
UG/KG
D Number: MH96
ANALYTE
CARBOXYLIC ACID
1 UNIDENTIFIED COMPOUND
lnorg Contractor: CHEM
Org Contractor: COMPU
Production Date: 10/15197 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08112/97 13:00
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACT ABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12434 FY 1997 Project: 97-0328
EXTRACT ABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC007SW MD Number: MK09
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: MK09
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:26
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12436 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC107SW
Media: SURFACEWA
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
Case Number: 25633
MD Number: MK11
D Number: MK11
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE (HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:26
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12435 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC007SD
Media: SEDIM
RESULTS UNITS
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
2500U
1000U
1000U
1000U
1000U
1000U
1000U
2500U
1000U
2500U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MK10
D Number: MK10
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 17:55
Ending:
RES UL TS UNITS ANALYTE
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
1000U
2500U
1000U
2500U
2500U
2500U
2500U
1000U
67
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12435 FY 1997 Project: 97 -0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC007SD MD Number: MK10
Media: SEDIM
RESULTS
1000JN
10000J
UNITS
UG/KG
UG/KG
D Number: MK10
ANALYTE
CARBOXYLIC ACID
5 UNIDENTIFIED COMPOUNDS
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08112/97 17:55
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R--qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12438 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC008SW
Media: SURFACEWA
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
Case Number: 25633
MD Number: MK13
D Number: MK13
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITRO BENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/9719:25
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12437 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC008SD MD Number: MK12
Media: SEDIM
RES UL TS UNITS
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
1200U
500U
500U
500U
500U
500U
500U
1200U
500U
1200U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MK12
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADI ENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
1200U
500U
1200U
1200U
1200U
1200U
500U
34
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO{A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
%MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12437 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC008SD MD Number: MK12
Media: SEDIM
RES UL TS UNITS
500JN UG/KG
D Number: MK12
ANALYTE
CARBOXYLIC ACID
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampllng and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12439 FY 1997 Project: 97-0328
EXTRACTABLE$ SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC 1 OSSO
Media: SEDIM
RESULTS
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
1200U
490U
490U
490U
490U
490U
490U
1200U
490U
1200U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MK14
D Number: MK14
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
1200U
490U
1200U
1200U
1200U
1200U
490U
33
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John McConney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/9718:45
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLOR0-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
e
•
EXTRACTABLES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA
Sample 12439 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC1 OSSO
Media: SEDIM
RESULTS UNITS
400JN UG/KG
Case Number: 25633
MD Number: MK14
D Number: MK14
ANALYTE
CARBOXYLIC ACID
lnorg Contractor: CHEM
Org Contractor: COM PU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
K-actual value is known to be less than value given. L-actua1 value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems; 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12441 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC009SW MD Number: MP51
Media: SURFACEWA D Number: MP51
RESULTS UNITS ANALYTE
10U UG/L 1,3-DICHLOROBENZENE
10U UG/L 1,4-DICHLOROBENZENE
10U UG/L 1,2-DICHLOROBENZENE
10U UG/L BIS(2-CHLOROETHYL) ETHER
10U UG/L HEXACHLOROETHANE
10U UG/L BIS(2-CHLOROISOPROPYL) ETHER
10U UG/L N-NITROSODI-N-PROPYLAMINE
10U UG/L NITROBENZENE
10U UG/L HEXACHLOROBUTADIENE
10U UG/L 2-METHYLNAPHTHALENE
10U UG/L 1,2,4-TRICHLOROBENZENE
10U UG/L NAPHTHALENE
10U UG/L 4-CHLOROANILINE
10U UG/L BIS(2-CHLOROETHOXY)METHANE
10U UG/L ISOPHORONE
10U UG/L HEXACHLOROCYCLOPENTADIENE (HCCP)
10U UG/L 2-CHLORONAPHTHALENE
25U UG/L 2-NITROANILINE
10U UG/L ACENAPHTHYLENE
10U UG/L ACENAPHTHENE
10U UG/L DIMETHYL PHTHALATE
10U UG/L DIBENZOFURAN
10U UG/L 2,4-DINITROTOLUENE
10U UG/L 2,6-DINITROTOLUENE
25U UG/L 3-NITROANILINE
10U UG/L 4-CHLOROPHENYL PHENYL ETHER
25U UG/L 4-NITROANILINE
10U UG/L FLUORENE
10U UG/L DIETHYL PHTHALATE
10U UG/L N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
10U UG/L HEXACHLOROBENZENE (HCB)
10U UG/L 4-BROMOPHENYL PHENYL ETHER
10U UG/L PHENANTHRENE
10U UG/L ANTHRACENE
10U UG/L DI-N-BUTYLPHTHALATE
10U UG/L FLUORANTHENE
10U UG/L PYRENE
10U UG/L BENZYLBUTYLPHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John McConney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:45
Ending:
UNITS ANALYTE
UG/L BIS(2-ETHYLHEXYL) PHTHALATE
UG/L BENZO(A)ANTHRACENE
UG/L CHRYSENE
UG/L 3,3'-DICHLOROBENZIDINE
UG/L DI-N-OCTYLPHTHALATE
UG/L BENZO(B AND/OR K)FLUORANTHENE
UG/L BENZO-A-PYRENE
UG/L INDENO (1,2,3-CD) PYRENE
UG/L DIBENZO(A,H)ANTHRACENE
UG/L BENZO(GHl)PERYLENE
UG/L 2-CHLOROPHENOL
UG/L 2-METHYLPHENOL
UG/L (3-AND/OR 4-)METHYLPHENOL
UG/L 2-NITROPHENOL
UG/L PHENOL
UG/L 2,4-DIMETHYLPHENOL
UG/L 2,4-DICHLOROPHENOL
UG/L 2,4,6-TRICHLOROPHENOL
UG/L 2,4,5-TRICHLOROPHENOL
UG/L 4-CHLORO-3-METHYLPHENOL
UG/L 2,4-DINITROPHENOL
UG/L 2-METHYL-4,6-DINITROPHENOL
UG/L PENTACHLOROPHENOL
UG/L 4-NITROPHENOL
UG/L CARBAZOLE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12440 FY 1997 Project: 97-0328
EXTRACTABLE$ SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC009SD
Media: SEDIM
RESULTS UNITS
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
1700U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
1700U UG/KG
670U UG/KG
1700U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
670U UG/KG
ANALYTE
Case Number: 25633
MD Number: MP50
D Number: MP50
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:30
Ending:
RESULTS UNITS ANALYTE
670U UG/KG BIS(2-ETHYLHEXYL) PHTHALATE
670U UG/KG BENZO(A)ANTHRACENE
670U UG/KG CHRYSENE
670U UG/KG 3,3'-DICHLOROBENZIDINE
670U UG/KG DI-N-OCTYLPHTHALA TE
670U UG/KG BENZO(B AND/OR K)FLUORANTHENE
670U UG/KG BENZO-A-PYRENE
670U UG/KG INDENO (1,2,3-CD) PYRENE
670U UG/KG DIBENZO(A,H)ANTHRACENE
670U UG/KG BENZO(GHl)PERYLENE
670U UG/KG 2-CHLOROPHENOL
670U UG/KG 2-METHYLPHENOL
670U UG/KG (3-AND/OR 4-)METHYLPHENOL
670U UG/KG 2-NITROPHENOL
670U UG/KG PHENOL
670U UG/KG 2,4-DIMETHYLPHENOL
670U UG/KG 2,4-DICHLOROPHENOL
670U UG/KG 2,4,6-TRICHLOROPHENOL
1700U UG/KG 2,4,5-TRICHLOROPHENOL
670U UG/KG 4-CHLORO-3-METHYLPHENOL
1700U UG/KG 2,4-DINITROPHENOL
1700U UG/KG 2-METHYL-4,6-DINITROPHENOL
1700U UG/KG PENTACHLOROPHENOL
1700U UG/KG 4-NITROPHENOL
670U UG/KG CARBAZOLE
51 % % MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12440 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC009SD
Media: SEDIM
RESULTS
900JN
2000J
UNITS
UG/KG
UG/KG
Case Number: 25633
MD Number: MP50
D Number: MP50
ANALYTE
CARBOXYLIC ACID
ALKANES
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:30
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12453 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC01 0SW
Media: SURFACEWA
RESULTS
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
25UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
25UJ
10UJ
25UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
Case Number: 25633
MD Number: MP63
D Number: MP63
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26, 1984)
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
25UJ
10UJ
25UJ
25UJ
25UJ
25UJ
10UJ
A-average value. NA-not analyzed. NAJ-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 09:40
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12454 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC010SD MD Number: MP64
Media: SEDIM
RES UL TS UNITS
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
1100U
430U
430U
430U
430U
430U
430U
1100U
430U
1100U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MP64
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
D1-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
1100U
430U
1100U
1100U
1100U
1100U
430U
24
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 09:25
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12429 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC011 SW
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
Case Number: 25633
MD Number: MJ01
D Number: MJ01
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAJ-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08112/97 18:25
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALA TE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-ANDIOR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12430 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC011 SD
Media: SEDIM
RESULTS UNITS
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
1200U
500U
500U
500U
500U
500U
500U
1200U
500U
1200U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MJ02
D Number: MJ02
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2.4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
500U
1200U
500U
1200U
1200U
1200U
1200U
500U
34
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/9718:45
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UGIKG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-ANDIOR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2.4-DIMETHYLPHENOL
2.4-DICHLOROPHENOL
2.4,6-TRICHLOROPHENOL
2.4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NA1-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLE$ SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA
Sample 12430 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC011 SD
Media: SEDIM
RESULTS UNITS
400JN UG/KG
Case Number: 25633
MD Number: MJ02
D Number: MJ02
ANALYTE
CARBOXYLIC ACID
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 18:45
Ending:
K-actua1 value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12420 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC012SW MD Number: MH92
Media: SURFACEWA D Number: MH92
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estlmated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/9711:12
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLOR0-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
e
•
EXTRACT ABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12421 FY 1997 Project: 97-0328
EXTRACTABLE$ SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC012SD MD Number: MH93
Media: SEDIM
RESULTS UNITS
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
1200U
490U
490U
490U
490U
490U
490U
1200U
490U
1200U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MH93
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-M ETHYLNAP HTHALE NE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE (HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
I norg Contractor: CH EM
Org Contractor: COMPU
RESULTS
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
490U
1200U
490U
1200U
1200U
1200U
1200U
490U
33
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John McConney
Requestor: PAT DEROSA
Project leader: DEROSA
Beginning: 08/12/97 11 :30
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4')METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12421 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC012SD
Media: SEDIM
RESULTS
200JN
600J
UNITS
UG/KG
UG/KG
ANALYTE
PINENE
Case Number: 25633
MD Number: MH93
D Number: MH93
1 UNIDENTIFIED COMPOUND
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 11 :30
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12431 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC013SW MD Number: MK06
Media: SURFACEWA D Number: MK06
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:35
Ending:
lnorg Contractor: CHEM
Org Contractor: COMPU
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
25U UG/L
25U UG/L
25U UG/L
10U UG/L
ANALYTE
BI8(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12432 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC013SD
Media: SEDIM
RESULTS
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
1100U
450U
450U
450U
450U
450U
450U
1100U
450U
1100U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: MK07
D Number: MK07
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE (HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
I norg Contractor: CH EM
Org Contractor: COMPU
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:50
Ending:
RESULTS UNITS ANALYTE
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
450U
1100U
450U
1100U
1100U
1100U
1100U
450U
27
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interterences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12432 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC013SD MD Number: MK07
Media: SEDIM
RESULTS UNITS
300JN UG/KG
D Number: MK07
ANALYTE
CARBOXYLIC ACID
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 16:50
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12419 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC014SW MD Number: MH91
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
1J
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
2J
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: MH91
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:45
Ending:
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
1J UG/L
25U UG/L
25U UG/L
25U UG/L
2J UG/L
10U UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is kn.own to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12418 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC014SD MD Number: MH90
Media: SEDIM
RESULTS UNITS
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
740U UGIKG
740U UGIKG
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
1900U UG/KG
740U UGIKG
740U UGIKG
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
1900U UG/KG
740U UG/KG
1900U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
740U UGIKG
740U UGIKG
D Number: MH90
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08112197 09:33
Ending:
lnorg Contractor: CHEM
Org Contractor: COMPU
RES UL TS UNITS
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
740U UGIKG
740U UGIKG
740U UGIKG
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
740U UGIKG
740U UGIKG
740U UG/KG
740U UG/KG
740U UG/KG
740U UG/KG
740U UGIKG
1900U UGIKG
740U UGIKG
1900U UG/KG
1900U UG/KG
1900U UG/KG
1900U UG/KG
740U UG/KG
56 %
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gtms: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12418 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC014SD
Media: SEDIM
RES UL TS UNITS
3000J UG/KG
ANALYTE
Case Number: 25633
MD Number: MH90
D Number: MH90
3 UNIDENTIFIED COMPOUNDS
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:33
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12427 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC015SW
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
Case Number: 25633
MD Number: MH99
D Number: MH99
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITRO BENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
01-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 11 :47
Ending:
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
25U UG/L
25U UG/L
25U UG/L
10U UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
01-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLOR0-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12428 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC015SD MD Number: MJ00
Media: SEDIM
RESULTS
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
1500U
600U
600U
600U
600U
600U
600U
1500U
600U
1500U
600U
600U
600U
600U
600U
310J
600U
600U
930
660
600U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MJ00
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITRO BENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 12: 15
Ending:
RES UL TS UNITS ANALYTE
600U
300J
600
600U
600U
1300J
490J
320J
600U
320J
600U
600U
600U
600U
600U
600U
600U
600U
1500U
600U
1500U
1500U
1500U
1500U
67J
45
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12428 FY 1997 Project: 97 -0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC015SD MD Number: MJ00
Media: SEDIM D Number: MJ0O
RESULTS UNITS
300JN UG/KG
200JN UG/KG
600JN UG/KG
ANALYTE
CARBOXYLIC ACID
ANTHRACENEDIONE
BENZOFLUORANTHENE (NOT B OR K)
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 12:15
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12433 FY 1997 Project: 97-0328
EXTRACTABLE$ SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC016SD MD Number: MK08
Media: SEDIM
RESULTS
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
2700U
1100U
1100U
1100U
1100U
1100U
1100U
2700U
1100U
2700U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MK08
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
1100U
2700U
1100U
2700U
2700U
2700U
2700U
1100U
69
A-average value. NA-not analyzed. NAl-interierences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 15:35
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resamp!ing and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12433 FY 1997 Project: 97 -0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC016SD
Media: SEDIM
RES UL TS UNITS
900JN UG/KG
4000J UG/KG
6000J UG/KG
Case Number: 25633
MD Number: MK08
D Number: MK08
ANALYTE
CARBOXYLIC ACID
ALKANES
3 UNIDENTIFIED COMPOUNDS
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 15:35
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12425 FY 1997 Project: 97-0328
EXTRACT ABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC017SW
Media: SURFACEWA
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
Case Number: 25633
MD Number: MH97
D Number: MH97
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE (HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:30
Ending:
lnorg Contractor: CHEM
Org Contractor: COMPU
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
25U UG/L
25U UG/L
25U UG/L
10U UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3'AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R--qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12426 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC017SD MD Number: MH98
Media: SEDIM
RESULTS
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
1000U
410U
410U
410U
410U
410U
410U
1000U
410U
1000U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
410U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MH98
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BI5(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/12/97 09:40
Ending:
lnorg Contractor: CHEM
Org Contractor: COMPU
RES UL TS UNITS
410U UG/KG
410U UG/KG
410U UG/KG
410U UG/KG
410U UG/KG
410U UG/KG
410U UG/KG
410U UG/KG
410U UG/KG
410U UG/KG
410U UG/KG
410U UG/KG
410U UG/KG
410U UG/KG
410U UG/KG
410U UG/KG
410U UG/KG
410U UG/KG
1000U UG/KG
410U UG/KG
1000U UG/KG
1000U UG/KG
1000U UG/KG
1000U UG/KG
410U UG/KG
20 %
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NA1-interferences. J-estimated value. N-presumptlve evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12412 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC018SW MD Number: LL02
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L ·
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: LL02
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 16:32
Ending:
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
25U UG/L
25U UG/L
25U UG/L
10U UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALA TE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12413 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
ld/Station:JC018SD MD Number: LL03
Media: SEDIM
RES UL TS UNITS
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
2300UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
2300UJ
910UJ
2300UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
910UJ
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: LL03
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
EXCESSIVE HOLDING TIME
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 17:35
Ending:
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS UNITS
910UJ UG/KG
910UJ UG/KG
910UJ UG/KG
910UJ UG/KG
910UJ UG/KG
910UJ UG/KG
910UJ UG/KG
910UJ UG/KG
910UJ UG/KG
910UJ UG/KG
910UJ UG/KG
910UJ UG/KG
910UJ UG/KG
910UJ UG/KG
910UJ UG/KG
910UJ UG/KG
910UJ UG/KG
910UJ UG/KG
2300UJ UG/KG
91 0UJ_ UG/KG
2300UJ UG/KG
2300UJ UG/KG
2300UJ UG/KG
2300UJ UG/KG
910UJ UG/KG
64 %
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA
Sample 12413 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC01 BSD
Media: SEDIM
RESULTS
40000J
10000J
UNITS
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: LL03
D Number: LL03
10 UNIDENTIFIED COMPOUNDS
ALKANES
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Production Date: 10/15/97 09:00
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 17:35
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number ls the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLE$ SAMPLE ANALYSIS EPA· REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12414 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC019SD
Media: SEDIM
RES UL TS UNITS
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
2000UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
2000UJ
780UJ
2000UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
120J
120J
780UJ
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
Case Number: 25633
MD Number: LL04
D Number: LL04
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
EXCESSIVE HOLDING TIME
lnorg Contractor: CHEM
Org Contractor: COMPU
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 17:50
Ending:
RES UL TS UNITS ANALYTE
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
780UJ
2000UJ
780UJ
2000UJ
2000UJ
2000UJ
2000UJ
780UJ
58
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12415 FY 1997 Project: 97-0328
EXTRACT ABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC020SW
Media: SURFACEWA
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
Case Number: 25633
MD Number: LL05
D Number: LL05
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11 /97 15:00
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA-REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12416 FY 1997 Project: 97 -0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC021 SW MD Number: LL06
Media: SURFACEWA D Number: LL06
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
_UG/L
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITRO BENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptlve evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 17:00
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
IN DENO (1 ;2,3-CD) PYRE NE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12417 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF Case Number: 25633
Id/Station: JC021 SD MD Number: MH89
Media: SEDIM D Number: MH89
RESULTS UNITS ANALYTE
soou UG/KG 1,3-DICHLOROBENZENE soou UG/KG 1,4-DICHLOROBENZENE soou UG/KG 1,2-DICHLOROBENZENE soou UG/KG BIS(2-CHLOROETHYL) ETHER soou UG/KG HEXACHLOROETHANE soou UG/KG BIS(2-CHLOROISOPROPYL) ETHER soou UG/KG N-NITROSODI-N-PROPYLAMINE
soou UG/KG NITROBENZENE soou UG/KG HEXACHLOROBUTADIENE soou UG/KG 2-METHYLNAPHTHALENE soou UG/KG 1,2,4-TRICHLOROBENZENE soou UG/KG NAPHTHALENE soou UG/KG 4-CHLOROANILINE soou UG/KG BIS(2-CHLOROETHOXY)METHANE soou UG/KG ISOPHORONE soou UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP) soou UG/KG 2-CHLORONAPHTHALENE
2000U UG/KG 2-NITROANILINE soou UG/KG ACENAPHTHYLENE soou UG/KG ACENAPHTHENE soou UG/KG DIMETHYL PHTHALATE soou UG/KG DIBENZOFURAN soou UG/KG 2,4-DINITROTOLUENE soou UG/KG 2,6-DINITROTOLUENE
2000U UG/KG 3-NITROANILINE soou UG/KG 4-CHLOROPHENYL PHENYL ETHER
2000U UG/KG 4-NITROANILINE soou UG/KG FLUORENE soou UG/KG DIETHYL PHTHALATE soou UG/KG N-NITROSODIPHENYLAMINE/DIPHENYLAMINE soou UG/KG HEXACHLOROBENZENE(HCB) soou UG/KG 4-BROMOPHENYL PHENYL ETHER soou UG/KG PHENANTHRENE soou UG/KG ANTHRACENE soou UG/KG DI-N-BUTYLPHTHALA TE soou UG/KG FLUORANTHENE soou UG/KG PYRENE soou UG/KG BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
soou soou soou
800U
800U soou soou soou soou soou soou
800U soou soou soou soou soou
800U
2000U soou
2000U
2000U
2000U
2000U soou
59
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 18:40
Ending:
UNITS ANALYTE
UG/KG BI5(2-ETHYLHEXYL) PHTHALATE
UG/KG BENZO(A)ANTHRACENE
UG/KG CHRYSENE
UG/KG 3,3'-DICHLOROBENZIDINE
UG/KG DI-N-OCTYLPHTHALATE
UG/KG BENZO(B AND/OR K)FLUORANTHENE
UG/KG BENZO-A-PYRENE
UG/KG INDENO (1,2,3-CD) PYRENE
UG/KG DIBENZO(A,H)ANTHRACENE
UG/KG BENZO(GHl)PERYLENE
UG/KG 2-CHLOROPHENOL
UG/KG 2-METHYLPHENOL
UG/KG (3-AND/OR 4-)METHYLPHENOL
UG/KG 2-NITROPHENOL
UG/KG PHENOL
UG/KG 2,4-DIMETHYLPHENOL
UG/KG 2,4-DICHLOROPHENOL
UG/KG 2,4,6-TRICHLOROPHENOL
UG/KG 2,4,5-TRICHLOROPHENOL
UG/KG 4-CHLORO-3-METHYLPHENOL
UG/KG 2,4-DINITROPHENOL
UG/KG 2-METHYL-4,6-DINITROPHENOL
UG/KG PENTACHLOROPHENOL
UG/KG 4-NITROPHENOL
UG/KG CARBAZOLE
% %MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J--estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. Li-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12417 FY 1997 Project: 97-0328
MISCELLANEOUS COMPOUNDS
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC021 SD
Media: SEDIM
RESULTS UNITS
900J UG/KG
ANALYTE
Case Number: 25633
MD Number: MH89
D Number: MH89
1 UNIDENTIFIED COMPOUND
lnorg Contractor: CHEM
Org Contractor: COMPU
A-average value. NA-not analyzed. NAl-interferences. J--estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/11/97 18:40
Ending:
K-actual value is known to be Jess than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane,,_
"
•
EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12457 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC001 PW
Media: GROUNDWA
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
Case Number: 25633
MD Number: MP68
D Number: MP68
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALA TE
lnorg Contractor: CHEM
Org Contractor: COMPU
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 20:15
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALA TE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
•
,.. EXTRACTABLES SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 10/15/97 09:00
Sample 12458 FY 1997 Project: 97-0328
EXTRACTABLES SCAN
Facility: JOHNSON CONTROLS GLOBE WINSTON-SALEM, NC
Program: NSF
Id/Station: JC002PW
Media: GROUNDWA
RESULTS
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
25UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
25UJ
10UJ
25UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
Case Number: 25633
MD Number: MP69
D Number: MP69
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26, 1984)
lnorg Contractor: CHEM
Org Contractor: COM PU
RESULTS
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
25UJ
10UJ
25UJ
25UJ
25UJ
25UJ
10UJ
Produced by: John Mcconney
Requestor: PAT DEROSA
Project Leader: DEROSA
Beginning: 08/13/97 21 :00
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UGIL
UGIL
UG/L
UG/L
UG/L
UG/L
UGIL
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-ANDIOR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of tech".ical chlordane
•