NC0001606250_20041209_Cristex Drum_FRBCERCLA C_Correspondence 1997 - 2004-OCR

MEMO TO: File
DATE: December 9, 2004
FROM: Jeanette Stanley, Environmental Chemist,
NC Superfund
SUBJECT: Cristex Drum Site
NCO 001 606 250
Oxford, Granville Co., NC
• F,/e,
I have reviewed the Cristex Drum Site ESI report, along with changes effective in the
Superfund Chemical Data Matrix (SCDM), effective January 2004. The June 2003 ESI report
recommended No Further Action Under CERCLA.
By applying the SCDM changes to the contaminants documented in the Observed Release
during the ESI, it appears that the Cristex Drum Site qualifies to receive further action under
CERCLA.
Based on this new inforrnation (updated SCDM), I recommend that the NFRAP
recommendation for the Cristex Drum site be removed, and that the site be recommended for
further action under CERCLA.
MEMO TO:
DATE:
FROM:
SUBJECT:
•
File
February 2, 2004
.Jeanette Stanley, Environmental Chemist,
NC Superfund
Cristex Drum Site
NCO 001 GOG 250
Oxford, Granville Co., NC
Spoke with Derr Leonhardt today, consultant for Cristex corporation (919) 621-5 832 ( cell).
He asked about the odds/ implications (CERCLA) of the Cristex site dropping out of the REC
program temporarily, until money can become available. Cristex corporation had been using lease
money from the warehouse for REC investigation fees, and the building has been vacant for some
time. The estate of Mr. Christensen was overseeing the cleanup, and was considering temporarily
exiting the REC program and then reentering it when the facility is again leased. He stated that
Cristex preferred to work under the REC program for remediation and did not want to risk losing
that ability.
I responded that the site was currently in the NFRAP status, but that it was a fairly high up
in potential CERCLA sites if the REC program fails to result in a cleanup. I responded that I could
not give a number of "odds" on the likelihood of Federal Superfund revisiting the site.
Mr. Leonhardt reported that the impoundment was still in place. Earthen berms had been
created to prevent overland 0ow into the impoundment. It was empty of water except for what fell
directly into. He reported that the investigation for other potential source areas underneath the
building had been completed and the report was due in another couple of months.
Mr. Leonhardt stated that Cristex had settled with A VTEX (adjacent JFD Channel Master
site) regarding groundwater remediation for any co-mingled groundwater. I suggested that he
investigate if temporary cessation of the REC activities would in any way jeopardize the settlement
with A VTEX, and do a cost/ benefit analysis of exiting and the re entering the REC program.
• • MEMO TO: John Powers, Hydrogeologist
DATE:
FROM:
SUBJECT:
NC Superfund ~
June 19, 2003 crcfU¥-.
Jeanette Stanley, Environmental Chemist
NC Superfund
Cristex Drum Site ·
NCO 001 606 250
Oxford, Granville Co., NC
!have completed reviewing the Environmental Assessment Report (October 2002) and the
Administrative Order on Consent (AOC). I have the following comments.
During the Environmental Assessment, it was determined that impacted soils remain in the
area adjacent to the drum storage pad, and further investigation to determine the vertical and lateral
extent of the VOC impact was recommended. The Work Plan (October 2002) describes plans to
investigate the extent of VOC contamination and to investigate SVOCs and metals in a Phase II plan
if required. During ES! sampling, one surface soil sample showed a number ofSVOCs detected at
levels less than quantitation limits. Also, metals results showed chromium, lead, nickel, vanadium,
and zinc at levels greater than three times background. Although the surface area of this soil has
been removed, and SVOCs and metals tend to be less mobile than VOCs, I suggest that this area of
remaining subsurface soil near the former drum storage pad also be investigated for metals and
SVOCs. The mobility of SVOCs and metals can be enhanced with VOC solvents.
Groundwater data from the Environmental Assessment showed several volatile organics at
levels greater than groundwater remediation goals (1,900 ug/L PCE, for instance). Note that the
quantitation limits for much of this volatile organic data was greater than the groundwater
remediation goal, leaving the possibility that groundwater is contaminated at levels above the
groundwater remediation goal, but less than the quantitation limit. For instance: for sample MW-I,
the quantitation limit was 5 ug/L whereas the 2L is 0. 7 ug/L. In MW-6, the quantitation limit for
vinyl chloride was 100 ug/L whereas the 2L is 0.015 ug/L, for trichloroethene it was al 100 ug/L,
whereas the 2L is 2.8 ug/L, etc . .In situations of high contamination, the laboratory must conduct a
number of dilutions which causes an increase in quantitation limits for all analytes, so this is
understandable in most cases. It is important to note; however, that the constituents showing a <l 00
ug/L, for example, does not document that a contaminant is less than 2L.
Subsurface soil collected from the hole for MW-9 in the interior of the building showed PCP.
Even though the groundwater sample did not show this contaminant, continued monitoring for 8270
SVOCs in at least some of the closer wells, and discussion of the SVOCs within the text of the report
. is important, at least for the CERCLA program. Data sheets showed that PCP was not detected in
the groundwater, but the report only discussed the SVOC ranges. If the data is available, a short
discussion of the results could.address potential future Superfund issues.
Page 5 and Appendix C of the Mid-Atlantic Associates, P.A., Phase I Remedial Investigation
Work Plan, Cristex Facility, October 2002 revealed that there are 5 residences using drinking water
wells within the 1/4 -1/2 mile target distance ring from the site. Are there plans to sample these
wells, or is this been adequately addressed under the JFD Electronics / Channel Master study?
Page_of_
SOL.WASTE MANAGEMENT DIVIS&
Receipt for Samples
SAMPLE COLLECTED SAMPLE TYPE DUPLICATE SAMPLE SAMPLE LOCATION
NUMBER OATE\TIME WATERlSOIL[OTHER OFRDiACPTiRJCTD ONSITEiOFFSITE
CtJ-z, ,-fL-1<~1z-,foo no< ✓ c----· ~ v----/
CO -;i. •iJ·-SL i~ I,"' J7z,/) , ___ ..----. ---'-/
(Y) -,). D f -SI i;: / ' 'rJV z.v /15U:::/-//
Co-:i..rL--5L lhilo0 ) <tfl<1 ;.,,,/ /
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.
c,I. (! tj 1l,.. I Po ,5J-, 1;/-t~/,. ""·"' ,l, /'is/; ':-1,.,/--s,;il ,/
[) c(, ,/_ if t.)£,, ~1,, 5,tJ l t..
I/
Receipt for the sarnple(s) described
above is hereby acknowledged:
Rece1pt/re1ect1on of duplicate or
split samples is hereby acknowledged:
Title
Comments:
(i\:\COCR.FRM)
~
Signature of Firm Owner, Operator,
or Agent
---------------------------------
SOU.ASTE MAt"\/AGEMENT DIVIS!.
Receipt for Samples
SAMPLE COLLECTED SAMPLE TYPE DUPLICATE SAMPLE SAMPLE LOCATION
NUMBER DATE:TIME WATER:soIL:OTHERiD OFRD:ACPTiRJCTD ONSITE:OFFSITE
c.o -;)., -1J '6' 1-1 u ! /r;Ji) ,/ ,✓ v v--
CO-lo\ -51) j 2-2 oa lo l r; ✓ v--v ..---
C'J--z.n-z.-~.;;) ' I v lo 45" ~ J/ 1,,,/
Co-·u2-Sp In ',11 ~ v--✓ v'
r'n-?-• :?> -fo) // 1 0 ,_.---' -1/ v-
O, ~:rS{) {J 3 O ✓ ,,,-v ' ----
CYJ 'J.o'f-SL /L(ou v---~ v I ,,-/
CID-:J.ofo-5D /4;_:o ~ L./ ✓ ' ----
Co -"1ntn-5 ~ I 0/1.0 ~ {../ ✓ ..---
CJ> --:2o1o-stt-l 14,TJ ✓-, ✓-l/ v--
r o-3-o!P-Sv-i /450 v--·-✓ ~
C,0-101 -5t>l 1,-I', ✓-,___... v---v
C1?-o1-01 -SD I trz.o v---,_.--I _.---,__...
C.V) -Z-1>i-SD 'ri. z-zlou /t,4C:--' ✓-----~ i.--' ~
C f) -l0)--5L ' I 5/zi/1J.1 ;ft;<
Receipt for the sample(s) descnbed
above is hereby acknowledged:
Rece1pt/reJccuon of duplicate or
split samples is hereby acknowledged:
Title
Signature of Firm Owner, Operator,
or Agent
~'Q.o!-
Title j
Comments: _________________________________ _
(A:\COCR.FRM)
MEMO TO FILE
DATE: July 24, 2000
FROM: Jeanette Stanley, Environmental Chemist,
NC Superfund
SUBJECT: Cristex Drum Site
NCO 00 I 606 250
Oxford, Granville Co., NC
•
On July 17, 2000, I visited the Cristex Drum site. I met Todd Tugwell, US Army Corps of
Engineers (COE) Regulatory Specialist (Raleigh Regulatory Field Office [phone] ext. 26).
I showed Todd the area below the surface impoundment that I thought to be a jurisdictional wetland.
I had previously received written permission from the property owner (Cristex Corporation) to enter
the property and delineate the wetland area. I provided a copy of this letter to Mr. Tugwell. Todd
stated that the 1989 wetland delineation manual discussed in the HRS guidance has since been found
to be a bit too broad, and that the US Army COE now uses the more conservative 1987 COE
definition of hydric soils.
Starting at the partial dam breech, Todd noted that the dam had mature trees growing in it.
He stated that this was a strong indication that the dam had been seeping for quite some time. At the
partial dam breech, Todd stated that the water in the impoundment and the pathway between the
wetland area were hydrologically connected. Todd began observation of the area and made the
following comments:
I. The wet area below the impoundment does not have a defined, jurisdictional channel,
The runoff pathway is braided.
2. The wet area below the impoundment definitely functions as a wetland.
3. Most vegetation is facultative, with a predominance of red maple and sweet gum
trees.
4. The hydrology of the area (water at surface, leaf litter along upgradient side of trees,
water in holes at a depth ofless than 12 ") is a strong indication of wetlands.
The first few augered holes did not show coloration that were strongly indicative of a wetland.
Mr. Tugwell indicated that mottling was present, and that a soil scientist would likely identify the soils
as hydric, but gong strictly by the color indicators on the Munsell chart, he could not confirm the
presence of of hydric soils at these points even though other wetland indicators were present. Mr.
Tugwell then located soils that matched coloration on the Munsell chart that were indicative of hydric
soils. He then proceeded to delineate the area of wetland below the surface impoundment by placing
flags around the perimeter. I stated that I would measure the perimeter of this wetland area when
I return to collect samples.
He located the point at which this wetland area drains into the perennial surface water
pathway. This was slightly upgradient from the culvert under the railroad track where the runoff from
the adjacent JFD/Channel Master site enters the perennial stream. Mr. Tugwell stated that the
wetland area was definitely hydrologically connected with this stream and that wetlands border this
stream on both sides, for a total width of about 5' until the area exits this wetland area at the small
dirt road near one of the monitoring wells for the JFD site.
e • U.S. ARMY CORPS OF ENGINEERS
Wilmington District
Action ID: 200021482 ----====~-----County: _____ G=ra,,,n"--v,__,i_,_,11-"e _______ _
NOTIFICATION OF JURISDICTIONAL DETERMINATION
Property
Owner ________ ~E=st~a~te'-o""f,._G=e-"or,.,g,,e'-C=hr~i-"st~e_,_,n-"se~n~-----------------
c/o Weinberger, Berman & Singer, P.C.
Address _______ ~A=tt-'-'n'--: ,,B"'a-'-'rry'-'--'S"'i"'n"'g"'e'--r ____________________ _
230 Park Avenue
New York NY 10169
Telephone Number ___ =2~12~-~9~49~-~7~6~00~--------------------
Size and Location of Property (waterbody, Highway name/number, town, etc.): This property is
located on the north side oflndustry Drive approximately 0.25 miles west of US 15 in Oxford, Granville
County, NC. The site is approximately 0.25 acres and located between a railroad bed and breached
holding pond.
Basis for Determination: The site contains a drained pond, wetlands, and a stream channel with
• indicators of ordinary high water marks, located adjacent to an unnamed tributary of Fishing Creek, above
headwaters, in the Tar River Basin.
Indicate Which of the Following Apply:
__K_There are waters of the U.S., to include wetlands, on the above described property which we strongly suggest
should surveyed. The surveyed wetland lines must be verified by our staff before the Corps will make a final
jurisdictional determination on your property.
__ Because of the size of your property and our present workload, our identification and delineation of your wetlands
cannot be accomplished in a timely manner. You may wish to obtain a consultant to obtain a more timely
delineation of the wetlands. Once the consultant has flagged a wetland line on the property, Corps staff will
review it, and, if it is accurate, we strongly recommend that you have the line surveyed. for final approval by the
Corps. The Corps will not make a final jurisdictional determination on your property without an approved survey.
__K_The waters of the U.S., to include wetlands, on your l~t have been delineated, and the limits of the Corps
jurisdiction have been explained to you. Unless there is a change in the law or our published regulations, this
determination may be relied upon for a period not to exceed five years from the date of this notification.
__ There are no waters of the U.S., to include wetlands, present on the above described property which are subject to
the permit requirements of Section 404 of the Clean Water Act (33 USC 1344). Unless there is a change in the law
or our published regulations, this determination may be relied upon for a period not to exceed five years from the
date of this notification.
Placement of dredged or fill materi\ii in wetlands on this property without a Department of the
Army Permit is in most cases a violation_ of Section 301 of the Clean Water Act (33 USC 1311). A
permit is not required for work on the property restricted entirely to existing high ground. If you
have any questions regarding the Corps of Engineers regulatory program, please contact
Todd Tugwell at telephone number (919) 876 -8441 extension 26
Project Manager Signature S ~ ~ :_ cY'1
Date July 19, 2000 ~bon Date July 19, 2005
SURVEY PLAT OR FIELD SKETCH OF THE DESCRIBED PROPERTY AND THE WETLAND
DELINEATION FORM MUST BE ATTACHED TO THE YELLOW (FILE) COPY OF THIS FORM.
Applicant: Estate of George Christensen
Attached is:
INITIAL PROFFERED PERMIT (Standard Permit or Letter of permission) A
PROFFERED PERMIT (Standard Permit or Letter of permission) B
PERMIT DENIAL C
X APPROVED JURISDICTIONAL DETERMINATION D
PRELIMINARY JURISDICTIONAL DETERMINATION E
SE@mI • wing ioeritifi cl 011tions regarcliiig an ailmiiiistratiye,,"1~-~
oecisio . ' . . . ~,
~omsr __
• ACCEPT: If you received a Standard Permit, you may sign the permit document and return it to the district engineer for final
authorization. If you received a Letter of Permission (LOP), you may accept the LOP and your work is authorized. Your
signature on the Standard Permit or acceptance of the LOP means that you accept the permit in its entirety, and waive all rights
to appeal the permit, including its terms and conditions, and approved jurisdictional determinations associated with the permit.
• OBJECT: If you object to the permit (Standard or LOP) because of certain terms and conditions therein, you may request that
the permit be modified accordingly. You must complete Section II of this form and return the form to the district engineer.
Your objections must be received by the district engineer within 60 days of the date of this notice, or you will forfeit your right
to appeal the permit in the future. Upon receipt of your letter, the district engineer will evaluate your objections and may: (a)
modify the permit to address all of your concerns, (b) modify the permit to address some of your objections, or (c) not modify
the permit having determined that the permit should be issued as previously written. After evaluating your objections, the
district engineer will send you a proffered permit for your reconsideration, as indicated in Section B below.
B: PROFFERED PERMIT: You may accept or appeal the permit
• ACCEPT: If you received a Standard Permit, you may sign the permit document and return it to the district engineer for final
authorization. If you received a Letter of Permission (LOP), you may accept the LOP and your work is authorized. Your
signature on the Standard Permit or acceptance of the LOP means that you accept the permit in its entirety, and waive all rights
to appeal the permit, including its terms and conditions, and approved jurisdictional determinations associated with the permit.
• APPEAL: If you choose to decline the proffered permit (Standard or LOP) because of certain terms and conditions therein, you
may appeal the declined permit under the Corps of Engineers Administrative Appeal Process by completing Section II of this
form and sending the form to the division engineer. This form must be received by the division engineer within 60 days of the
date of this notice.
C: PERMIT DENIAL: You may appeal the denial of a permit under the Corps of Engineers Administrative Appeal Process
by completing Section II of this form and sending the form to the division engineer. This form must be received by the division
engineer within 60 days of the date of this notice.
D: APPROVED JURISDICTIONAL DETERMINATION: You may accept or appeal the approved JD or
provide new information.
• ACCEPT: You do not need to notify the Corps to accept an approved JD. Failure to notify the Corps within 60 days of the
date of this notice, means that you accept the approved JD in its entirety, and waive all rights to appeal the approved JD.
• APPEAL: If you disagree with the approved JD, you may appeal the approved JD under the Corps of Engineers Administrative
Appeal Process by completing Section II of this form and sending the form to the division engineer. This form must be received
by the division engineer within 60 days of the date of this notice.
E: PRELIMINARY JURISDICTIONAL DETERMINATION: You do not need to respond to the Corps
regarding the preliminary JD. The Preliminary JD is not appealable. If you wish, you may request an
approved JD (which may be appealed), by contacting the Corps district for further instruction. Also you may
provide new information for further consideration by the Corps to reevaluate the JD.
l~J;'.~ill.l~Wml~~l!/&S11Y!i!l>R¥it~i:P&~!-,1illi\i>.!3:Jl;!j);f!~:t:lllii1:.W!ffl-lm!.IID.tir~FJiJ?R:gfill~Jt:1Uvll~
REASONS FOR APPEAL OR OBJECTIONS: (Describe your reasons for appealing the decision or your objections to an
initial proffered pcnnit in clear concise statements. You may attach additional information to this form to clarify where your reasons
or objections are addressed in the administrative record.)
•
ADDITIONAL INFORMATION: The appeal is limited to a review of the administrative record, the Corps memorandum for the
record of the appeal conference or meeting, and any supplemental information that the review officer has determined is needed to
clarify the administrative record. Neither the appellant nor the Corps may add new information or analyses to the record. However,
you may provide additional information to clarify the location of information that is already in the administrative record.
m@J:hlif.i..(i)FJ@0~Tn'!lfil@Rl~illES.illI©~Sl~~~R:B.'~1iL<i21\!~fiF ■llil111111
If you have questions regarding this decision and/or the appeal If you only have questions regarding the appeal process you may
process you may contact: also contact:
Mr. Todd Tugwell, Regulatory Specialist Mr. Arthur Middleton, Administrative Appeal Review Officer
Raleigh Regulatory Field Office CESAD-ET-CO-R
6508 Falls of the Neuse Road, Suite 120 U.S. Army Corps of Engineers, South Atlantic Division
Raleigh, North Carolina 27615 60 Forsyth Street, Room 9M 15
Atlanta, Georgia 30303-880 I ~ -
RIGHT OF ENTRY: Your signature below grants the right of entry to Corps of Engineers personnel, and any government
consultants, to conduct investigations of the project site during the course of the appeal process. You will be provided a 15 day
notice of any site investigation, and will have the opportunity to participate in all site investigations.
Signature of appellant or agent.
DIVISION ENGINEER:
Commander
U.S. Army Engineer Division, South Atlantic
60 Forsyth Street, Room 9MIS
Atlanta, Georgia 30303-3490
Date:
-
Telephone number:
DATA FORM • ROUTINE WETLAND DETERMINATION
(1987 COE Wetlands Determination Manual)
Project/ Site Estate of George Christensen/ Indust[Y Dr. , Oxford Date: 7-I 8-00
Applicant/ Owner: NC SuQerfund Section County: Granville
Investigator: Todd Tu•well State: NC
Do normal circumstances exist on the site? Yes _x_ No __ Community ID: UP
Is the site significantly disturbed (Atypical situation)? Yes ---No _x_ Transect ID:
Is the area a potential problem area? Yes ---No _x_ Plot ID: 2
(explain on reverse if needed)
VEGETATION
Dominant Plant Species Stratum Indicator Dominant Plant Species Stratum Indicator
1. Acer rubrum TR FAC 8. Eulalia viminea HR FAC+
2. Pinus taeda TR FAC 9. Toxicodendron radicans VI FAC
3. Acer rubrum SA FAC 10. Camesis radicans VI FAC
4. Forestiera ligustrina SA FAC 11. ---5. Lig_uidambar sty__raciflua SA FAC+ 12.
6. Forestiera ligustrina SA FAC 13.
7. Boehmeria cylindrica HR FACW+ 14.
TR:: Trees (non-climbing woody plants,~ 3.0 in. DBH) HR= Herbs (non-woody plants & woody plants,< 3.2 ft.,< 3.0 in. DBH)
SS =Saplings/ Shrubs (woody plants,~ 3.2 ft.,< 3.0 in. DBH) VI = Vines (woody climbing vines,~ 3.2 ft.)
Percent of Dominant Species that are OBL, FACW, or FAC excluding FAC-). 100%
Remarks:
HYDROLOGY
--Recorded Data (Describe In Remarks): Wetland Hydrology Indicators
__ Stream, Lake, or Tide Gauge
__ Aerial Photographs Primary Indicators:
Other --Inundated --__ Saturated in Upper 12"
_x_ No Recorded Data Available --Water Marks
_x_ Drift Lines
Field Observations: __ Sediment Deposits
_x_ Drainage Patterns in Wetlands
Depth of Surface Water: 0 (in.) Secondary Indicators:
__ Oxidized Roots Channels in Upper 12"
Depth to Free Water in Pit: 0 (in.) --Water-Stained Leaves
__ Local Soil Survey Data
Depth to Saturated Soil: 17 (in.) --FAC-Neutral Test
__ Other (Explain in Remarks)
Remarks: There were a drift lines along with small drainage patterns. However, the data point was located near
a stream bed.
•
SOILS
Map Unit Name
(Series and Phase): Appling sandy loam Drainage Class: well-drained
Taxonomy (Subgroup): Typic Kanhapludults Confirm Mapped Type? Yes --No --
Profile Descri[!:tion:
Depth Matrix Colors Mottle Colors Mottle Texture, Concretions,
(inches} Horizon (Munsell Moist} (Munsell Moist} Abundance/Contrast Structure etc.
0-6 A lOYR 5/4 none ------------------clav
6-12 B lOYR 5/4 7.5YR 4/6 many/distinct sandy clay
12+ C lOYR 5/6 none -------sand)'.
Hydric Soil Indicators:
Histosol Concretions ----
__ Histic Epipedon __ High Organic Content in Surface Layer in Sandy Soils
--Sulfidic Odor __ Organic Streaking in Sandy Soils
__ Aquic Moisture Regime __ Listed On Local Hydric Soils List
__ Reducing Conditions __ Listed on National Hydric Soils List
__ Gleyed or Low-Chroma Colors __ Other (Explain in Remarks)
Remarks:
WETLAND DETERMINATION
Hydrophytic Vegetation Present?
Wetland Hydrology Present?
Hydric Soils Present?
Remarks:
Yes _x__ No
Yes_x__ No
Yes No_x__
Is the Sampling Point
Within a Wetland? Yes __ No_x__
DATA FORM • ROUTINE WETLAND DETERMINATION
(1987 COE Wetlands Determination Manual)
Project/ Site Estate of George Christensen/ Industrx Dr. Oxford Date: 07-18-00
Applicant/ Owner: NC Sugerfund Section County: Granville
Investigator: Todd Tugwell State: N.C.
Do normal circumstances exist on the site? Yes _x_ No --Community ID: Wet
Is the site significantly disturbed (Atypical situation)? Yes --No _x_ Transect ID:
Is the area a potential problem area? Yes --No _x_ Plot ID: I
(explain on reverse if needed)
VEGETATION
Dominant Plant Sgecies Stratum Indicator Dominant Plant Species Stratum Indicator
1. Acerrubrum TR FAC 8.
2. Liguidambar s!J!._raciflua TR FAC+ 9.
3. Acerrubrum SA FAC 10.
4. Liguidambar s!J!._raci(J_ua SA FAC+ 11.
5. Eulalia viminea HR FAC+ 12.
6. lonicera iaaonica VI FAC-13.
7. Toxicodendron radicans VI FAC 14.
TR= Trees (non-climbing woody plants,~ 3.0 in. DBH) HR= Herbs (non-woody plants & woody plants,< 3.2 ft.,< 3.0 in. DBH)
SS =Saplings/ Shrubs (woody plants,<:! 3.2 ft.,< 3.0 in. DBI-I) YI = Vines (woody climbing vines, ~ 3.2 ft.)
Percent of Dominant Species that are OBL, FACW, or FAC excluding FAC-). 85%
Remarks:
HYDROLOGY
--Recorded Data (Describe In Remarks): Wetland Hydrology Indicators
__ Stream, Lake, or Tide Gauge
__ Aerial Photographs Primary Indicators:
Other --Inundated --_x_ Saturated in Upper 12"
_x_ No Recorded Data Available --Water Marks
_x_ Drift Lines
Field Observations: __ Sediment Deposits
_x_ Drainage Patterns in Wetlands
Depth of Surface Water: 0 (in.) Secondary Indicators:
__ Oxidized Roots Channels in Upper 12"
Depth to Free Water in Pit: 6 /in.) _x_ Water-Stained Leaves
__ Local Soil Survey Data
Depth to Saturated Soil: 0 (in.) --FAG-Neutral Test
__ Other (Explain in Remarks)
Remarks:
• SOILS
Map Unit Name
(Series and Phase): Appling Sandy Loam Drainage Class: well-drained
Taxonomy (Subgroup): Typic Kanhapludults Confirm Mapped Type? Yes --No --
Profile DescriQtion:
Depth Matrix Colors Mottle Colors Mottle Texture, Concretions,
(inches) Horizon (Munsell Moist) (Munsell Moist) Abundance/Contrast Structure. etc.
0-6 A 2.5YR 3/2 I0YR 4/6 common/distinct sandy clay
6-18 B 2.5YR 5/2 I0YR 4/6 common/distinct sandy cla)'.
18+ C I0YR 4/3 none sandy
Hydric Soil Indicators:
--Histosol --Concretions
__ Histic Epipedon __ High Organic Content in Surface Layer in Sandy Soils
--Sulfidic Odor __ Organic Streaking in Sandy Soils
__ Aquic Moisture Regime __ Listed On Local Hydric Soils List
__ Reducing Conditions __ Listed on National Hydric Soils List
..L Gleyed or Low-Chroma Colors __ Other (Explain in Remarks)
Remarks:
WETLAND DETERMINATION
Hydrophytic Vegetation Present?
Welland Hydrology Present?
Hydric Soils Present?
Remarks:
Yes_x_ No
Yes_x_ No
Yes_x_ No
Is the Sampling Point
Within a Wetland? Yes_x_ No __
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• NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
July 17, 2000
Barry Singer, Esq.
Weinberger, Berman & Singer
230 Park Ave.
NewYork,NewYork 10169
RE: Cristex Drum
NCO 001 606 250
Industry Drive
Oxford, Granville County, NC
Dear Mr. Singer:
DIVISION OF WASTE MANAGEMENT
As 1 understand, you represent the Cristex Corporation, P.O. Box 527,
Allenwood, NJ 08720. I am writing this letter to request permission to enter the
property in order to delineate any wetland areas on the northern part of the property. 1
hope to get your client's permission today for a visit tomorrow. I apologize for the short
notice, but I contacted the US Army Corps of Engineer wetland expert for the Oxford
area, thinking that we would arrange a time within the next month or two. He will be in
the area tomorrow, July 18, 2000, but will not be available again for another 6 - 7 weeks.
No samples will be collected tomorrow. We will simply be looking at the
vegetation and soils to determine if wetland areas exist. Your client will receive a letter
from the COE to verify any wetlands found. Please provide the correct address if the
above is incorrect. This wetland delineation is a preliminary step of a planned Expanded
Site Inspection (ES!) on the Cristex property. We understand that you may be proposing
the clean up of the surface impoundment and possibly other contaminated areas on the
property. We need to document site conditions using CLP-quality data before any
cleanup proceeds.
As part of the ES!, and pending observations made on the site tomorrow, we plan
to collect 14 soil/sediment and IO surface water samples on the site and have these
analyzed for VOCs, SVOCs (including PCBs) and TAL metals. We tentatively plan to
collect these samples on August 22, using one sampling team. lfyou wish to collect split
samples, you will need to provide your own sampling jars and have a consultant present
to receive and label these samples. lfyou have any questions, you may contact me at
[phone] ext. 318.
S01i Vi((_ fflx tv:
L;.,,1z)g '-/'f -(,1~7.__
K.,. >fJIVJ-(,. C\ 11-u. L ~ J
Sincerely,
.J/=c--ll-r-,
anette
Environmental Chemist
NC Superfund Section
1646 MAIL SERVICE CENTER, RALEIGH, NORTH CAROLINA 27699-1646
401 OBERLIN ROAD, SUITE 150, RALEIGH, NC 27605
PHONE 919-733•4996 FAX [phone]
AN EQUAL OPPORTUNITY/ AFFIRMATIVE ACTION EMPLOYER -50% RECYCLED/IC% POST-CONSUMER PAPER
07/17/00 1J: 11 FAX [phone] \\'EI NBERGER-BERl! • •
WEINBERGER, BERMAN & SINGER, P.C.
H::irry Singer
Via Fax
230 PARK AVENUE, Nl:.W YOKK, N.EW YORK 10169
T.t.LhPHONE; (212) 9'i9-7600 FAX: {21:2) 949-fi162
July 17, 2000
Ms. Jeanette Stanley
Environmental Chemist
NC Superfund Section
North Carolina Oepartment of
Environmental and Natural Resources
1646 Mail Service Center
Raleigh, North Carolina 27699-1946
Re: Estate of George Christensen, Oeceased
Cristex Facility. Oxford. North Carolin~
Dear Ms. Stanley:
In response to your fax to me of July 17, 2000, please be
advised that you have permission to enter the Cristex property
tomorrow in order to delineate any wetland areas on the northern
part of the property.
If you have any questions concerning the foregoing, please
telephone me.
enc.
~002
07/17/00 13:10 FAX [phone] WEINBERGER-BERM • •
WEINBERGER, BERMAN & SINGER, P.C.
2JC PARK AVENUE, NEW YORK. NEW YORK t:169
TELEPHONE: (212) 9•9-7600 FAX: [phone]
DATE:
PLEASE DELIVER IMMEDIATELY TO J/4; i2Ly
TOTAL NUMBER OF PAGES (INCLUDING THIS PAGfu eJ.
WE ARE TRANSMITTING FROM CANON FAX 61 O{G-3)
ANY PROBLEMS IN RECEIVING PLEASE CALL BACK AS SOON-AS
POSSIBLE.
TELECOPIER SENDER, E7 ~ ,
RECEIVER'S TELECOPIER NUMBER IS: 91 o/ ~rJ j 3 · ff/I
COMMENTS: __________________ _
IBIS MESSAGE IS IJ',TE:,."DED ONLY FOR 1HE USE OFTJ IE IND MD UAL OR ENTITY TO WHICH IT IS ADDRESSED, AND
MAY CONTAIN INFORMATION TIIAT IS PFJVJI.EGED, CONFIDEi'ITIAL M"D EXEMPT FROM DISCLOSURE U:,."DER
AFPLJCAllLE 'J>.W. IF Tim RfAD!oR OF TR,.; MESSAGE IS NOT THE INTENDED RECIPIENT OR TI-lE EMPLOYEE OR
AG!ll'ff RESPONSIBLE FOR DELJVERING TI IE MESSAGE TO IBE INTENDED RE□PIE!,T, YOU ARE HEREBY NOTIFIED
TIIAT ANY DISSE.\!1NATION, DISTRl□ UTJ
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YOU HA VE RECEJVED 1HIS COMMUNICA'!lON IN ERROR. PLEASE NOTIFY US IM.\IEDIATEL Y BY TELEFHONE AND
KEl1JRN THE ORIGINAL MESSAGE TO liS ,\T TllE AfJOVE ADDRESS Vu\ THE U.S. POSTAL SER\~CE. TI!ANK YOU.
~001
SITE HEALTH AND SAFETY PLAN
A. General Information
•
Site Name c.r:.is_t,ex_ _______________ ID # N.C.O_Q0.1_6..0-6_25._Q __
Location ,Co_rnor of Indust.riaLD.L and Pine Tree
Rd,_ilicf_ard,__Gran.tille_Counj;y..,__N;.__ __
Proposed Date of Investigation ]j_JJL_t_o_a/..1_8_,12Jl,-"--',__ ___ _
Date of Briefing _1/_.1J_/_2_o_o_o, _______________ _
Date of Debriefing BL2.l/_2_0_o_o, ______________ _
Nature of Visit (check one) On-Site Reconnaissance
Off-Site Reconnaissance
Sampling
Sampling Overview
Remediation Overview
_x_
Health Department Official Contacted Mr:._MLt.chell_Arnou.i.,._ _______ _
Date of Contact _July_ll,_2_QQ_Q, ______________________ _
Site Investigation Team: All site personnel have read the Site Health and
Safety Plan and are familiar with its provisions.
e_ers_onnel Resp_an s i bi J ities Si_gnat._ure
Team l J_e_an_e_t_t._e_S_t._anle,,_ __ _t_e.am 1 eader _r:_e.c..on_ ~Jtc~
Plan Preparation:
Prepared By, David I.i lleJL,Jndus_tr:Lal_Hy:gLene_r:nnfilllt.ant
Reviewed By: J__ac_k______B_u.t..1.e.r..,_S.up.er.f.un.d_S_e.c.ti~_hi.!
•
B. SITE/WASTE CHARACTERISTICS
Waste Type(s) _X_Liquid _lL_Solid ___ Sludge ___ Gas _x__vapor
Characteristics ___ Corrosive ~Ignitable ___ Radioactive
_x_volatile __x_Toxic Reactive Other
List Known or Suspected Hazards (physical, chemical biological or
radioactive) on Site and their toxicological effects. Also, if known, list
chemical amounts
HAZARD
Te.ttachLor:o_e_t_hen.~----
Xy_l_en~----------
Chr.o_mi.u .. ~---------
Lea~-----------
Mtlh:,,:l_ene_clll_o_r_i_d ___ _
Ethy_l_b_e_n_z_en, _______ _
.TrJ~hloroethY-~l~e~o~e,_ ___ _
WARNING PROPERTIES
_Qdo_r_Thr:e_shold_l_QIJ---=----4__,_6Jl~.Q_ppm
____ __\,J__.L_a=s__J(L 17 -40 PP•~-----
---~_>T...:__(L_Q5_-_2_Q0_pp,"~----
----~O~T~-~oo_dat~--------
----=~~lliLdat~--------
----~-a_ctat~--------
O.T-=-25.c_3.0_ppm_(.c_an_actap_t__t_o___octru:L_
OT - O 25 -200_ppm ____ _
_ ___ >T...:__(L_2_-_4__Q_Q_pp .. ~----
UNDERGROUND UTILITIES CHECKLIST
EXPOSURE
LIMIT
2_5_ppm_
_5_0_ppm _
ifil)_ppnL
.0 .•. 5-mgLm:
_a __ a_i_mgLm:
D~O_S_mgLm:
2_5_ppm_
],,_QO_ppnL
_5_0_ppm_
lltili_t:,,: Lo_c_ator/Contact ___ Ee.rs.an !'hone_# Date_o_f_Lo_c_a_t_i_an
Power
Telephone
Gas
Water
Sewer
Call_made..h:,,:,
2
ID # NC_0_0_0.1_6.0.6_25 _______ _
Facility Description: Size _unknuwn __ Buildings --~nknQW,~-----
Disposal Methods Being Investigated BID:ied_dr.ums_. _____________ _
Unusual Features on Site (dike integrity, power lines, terrain, etc.)
11Qllie_k,ruUWJ,L__ ____________________________ _
History of the Site, l'h_e_sit.e_was_a_forme.r__t.extile_milLand_the_dr_ums_wer.e
dis.c.o.v~_while_=nduc.ting_a_s.il:.e. vis it t o_J:ED_El.e.ct=i..c.~--------
C. HAZARD EVALUATION
Ihe_sit_e_can_be_t.oured_irLl.e.v.e.LD_p=.t.e.c.tion .. _No_sampling_wi.LL_b,.._,====
Steel toed work___boo_t._s__wi lJ be wo.rn_wbi 1 e t.o..urin_g_ .CQnduc.t.ed_a t t bi s_tirne
t.h_e_site. --============================
Map or Sketch Attached?
D. WORK PLAN INSTRUCTION
->"'-~----
Perimeter Identified?
Command Post Identified? no ____ _
Zones of Contamination Identified? no, ____ _
Personal Protective Equipment/Level of Protection: ___ c
Modifications
3
_x_D
Surveillance Equipment:
HNU
OVA
Explosimeter
Decontamination Procedures
•
ID # NCD__Q_QJ__6_Q_IL_251)~------
Detector Tubes and Pumps
02 Meter
Radiation Monitor
_____ Level C Respirator wash, respirator removal, suit wash (if needed),
suit removal, boot wash, boot removal and glove removal.
__ X __ Level D Boot wash and rinse and boot removal, suit removal, glove
and goggle removal.
Modifications Disp_os_e_o_f_t_r_ash_p.r_op_er.ly_,_on.=.s.i.t.e_ti_p_ossible_, ______ _
Work Sc hed u 1 e /Vis i t Obj e ct i ve s The_purp_os_e_of_this_vJ.sit_i,s_1:Q____cJ,_e_t__e_rmin_e_
iLthe_s.i.t.e_pos.es__a_threat to the public heal t.h_o_r_enyJ.ronmenLb.ecaus_e__of
r.e.l.P-ases of cont..aminan.t.s_t_o_s..o.il,_s_urf.a_c.e_w.a..t.er..,_gr.o_undw.at..e.L or ai.r:...====
No___s_ampli11_g--"lill be condu.c..t..e.d....aLtbis__t_i,=~----------------
EMERGENCY PRECAUTIONS
Ro.u.t_e_oLExp_os.ur.e
Ey_es _______________ _
s. .
lnhalal:.io,~----------
lng.e"-C.....U.Ll_ ___________ _
4
E'.irs_LAid
irri_ga_t_e_immedia~t~e~J...,y,_ _______ _
aoap_aruLwa.t.er_was. _________ _
f.r_e_sh_ai.r_and__ arti fi ci al r..e_spiration
ge.Lmedi cal at t.ention_imme.diat.tly __
•
Location of Nearest Phone: unkrullin____lny____r_eaideru:;_es_Lbus.in_e_s_s_e_s_?~~====
Hospital (Address and Phone Number)
Grarudlle_MedkaLCen.ter_ Col l egP_&,Jxtent i on,_EQ_Bo~!M'?_,_Qx£ouL~N~C'==
Jil9-)_62J~_ -_can_handle._ch.emi_cally_c_ontaminated_pati.ents.========
Emergency Transportation Systems (Phone Numbers)
Fire _(9.19-)__69_°-=.3-0.0"'==============
Ambulance Jllil_li9J2.=.JJlJl"'=============
Rescue Squad _(9_19J--69-0~0-.===========~
Emergency Route to Hospital Iak.e...J:he_ac_c_es_s__roa.cLbac!Lt_a_SJL.L0.M.., t~i~i~r~n~==
ri.ghL_an.cLatay_on_SR_J.Dfil__t,o_Rout.e.J.5./.J.5Jl.L9.Land. .. __t_urn-1tlt Irav_e,LDDtlh=
approx.imately..-Lmile.,_the_hosp.i.tal_will_b_e_on_the_r.ight_,==========
PREVAILING WEATHER CONDITIONS AND FORECAST ________________ _
EQUIPMENT CHECKLIST
___ Air purifying respirator
Cartridges for respirator
Eye Wash Unit
HNU
__ X_ OVA
Explosimeter
Radiation Monitor
__ x_ Decontamination
Materials
__ x__ First Aid Kit
__ X_ 3 gal. Deionized H20
Rain suit
Gloves ( PE/EY..C/ni_t.r.i.l.e/cloth)
Billl.ts/Boot Covers_
__ x__ Coveralls (~Ls.aranex)
__ x_ Eye Protection (go.ggle.s/shi_eldl
__ X_ Hard Hat
STATE POISON CONTROL CENTER
1-800-848-6946
safeform.323d 5
• •
TO BE COMPLETED BY PROJECT MANAGER
PROJECT MANAGER: .Ie,.\ne.t_t_e__~tanlay __
INVESTIGATION DATE: ]j_l_B~t.D__B_fil_,I_JJ~--
RECONNAISSANCE _X_ SAMPLING VISIT ___ REMEDIATION/SAMPLING OVERVIEW
Respirator Worn By Approximate Time in Respirator
Air Monitoring Data (Include Calibration Reading)
HNU:
OVA:
Explosimeter:
Radiation Meter:
Were there any injuries? If yes, explain: ______________ _
If the maximum personal protective equipment as outlined in the Hazard
Evaluation Section was not used, please justify:
Visitors Present Organization Represented
Signature
:CFC Pesticide
Hspo~al
,ICO 986 180 883
!FD Electronics
Channel Master)
1cr,--.'2 263 02s
17'30"
• • \VEINBERGER, BER.MAN & SINGER P.C.
K~rry Sir.gcr
Via Fax
n:: P.'-.R..K AVE.;'l"._7£, :-.·.::.w ':'OK.K.. ;\:.I::\\' :'ORK ::if9
'ftLU'HO'.'\'L ;2!2) 9•9-7(;(;,'.: :::AX: ;2:'..'.; 749-filfi2
July 17, 2000
Ms. Jeanette Stanley
Environmental Chemist
NC Superfund Section
North Carolina Departme~t of
Environmental and Natural Resources
1646 Mail Service Center
Raleigh, North Carolina 27699-1946
Re: Esta~e of George Ch~istensen, Deceased
Cris~ex ?acility, Oxford, North Carolina
Dear Ms. Stanley:
In response to your fax to me of July 17, 2000, please be
advised that you have permission to enter the Cristex property
tomorrow in order to delineate any wetland areas on the northern
part of the property.
If you have any questions concerning the foregoing, please
telephone me.
enc.
Federal •
• Trip Notification & Authorizat1...,o
Prepared by: r $fav'\f ft
• Use O!ack Ink or Typewriter only-Staff to fill out first:! blocks only.
Site Trip.
DateofTrip: 7-{g' .Jo '?-{~-VO
If trip date changed or cancelled note below:
Trip Date Changed To: ____ Cancelled:
NCD#: Site Name: C n-.sfcx,
Orno.1, -;; ~ City: County:
Reason for Trip: £.5 / ~ {CTr\_,,;
. Name of Hotel (Overnight Trip): Mlf Hotel Telephone Number: ( ) -~,!-"-'------
Authorized by:
Project Team Leader: ,--s:-sf¾ I flf;.
Assistants: T.1y._Bo\~(5W\{f), ________________ _
Attach To Notification Form: 1 copy each:
Submit to the
Industrial Hygienist
Preliminary Assessment Form (First page only)
Site Map
PA Transmittal Letter
(!'lease list appropriate County Health Department contact pcr.;on 10 eall to adv;sc of trip) . ! 1 /J Gv, 1/eiZJ
Environmental Supervisor or Health Director to call: fn if-cle,d f1Idolf Title: <£;:"'191/Vrs,,,,
Notes:
(Note if Or., M.l'., etc.)
Telephone Number: Qs::J) $_~ ..S--..)~_s
Health Department Official Contacted: or,!JL6f/4r:/lo!I
Back Up Letter Required: Yes __ No _L.
/1,ft,t,Gr/ ((V, 4r-,v;/) 7-l>-D0 {/J.it)
Note: Si~cd ori~nal to Daia Manc1:,.:cr
• Federal •
Trip Notification & Authoriz?tiv/1
Site Trip.
Date of Trip: &o/ / .-S / 1 ~"'c;)
J If trip date changed or cancelled note below:
Trip Date Changed To: ____ Cancelled:
NCO#: !Vtu ovl VO ii ~S-0
City: ()xfav/
Site Name: Cr,;fK Prlf1V\ --=----,----'--
County: (J revn vr//f,
Reason for Trip:
Today's Date:]/;~@0
Name of Hotel (Overnight Trip): Hotel Telephone Number: ( ) --------
Authorized by:
Project Team Leader: ~tc= I e 1; .
Assistants: -:r::i:;C\ te StiA_
Attach To Notification Form: 1 copy each: Preliminary Assessment Form (First page only)
Submit to the Site Map
Industrial Hygienist PA Transmittal Letter
(Please 1;51 appropriate County Health Department contact pmon to call to advise of trip)/1, { ·ft b/\ </,
Environmental Supervisor or Health Director to call: t.l('f,~[;t ,J(lo/jTitle: ~,/is0 r
Notes:
(Note if Dr., M.I'., etc.) ~
Telephone Number: (~if'/:;__ --5 -<C3
Health Department Official Contacted: (r);{cJef/ ,/tNI/
Back Up Letter Required: Yes __ No _,L'
lvo--rC.eJ .t{)r, J}rfl/J/J )-, ;> -oo (..08(,)
Note: Si)!ncd ori~na! to Data Mana~cr ·
• •
MEMO TO FILE
March 3, 2000 9 ~
Jeanette Stanley, Environmental Chemist, --{i, ri)><,
NC Superfund {,{J1£{//I~ C_J
Cristex Drum Site
NCO 001 606 250 .
DATE:
FROM:
SUBJECT:
Oxford, Granville Co., NC
Today, I spoke with Derr Leonhardt, Leonhardt Consulting [phone], consultant for
Cristex Drum. I told him that I have completed reviewing the December 28, 1999 Remedial
Investigation Work plan for the facility that was prepared by Mid-Atlantic Associates. This Work
plan was received by NC Superfund Section on February 16, 2000.
I reiterated to Mr. Leonhardt that per Mid-Atlantic's statement in the introduction of this
Work plan, NC may or may not recognize the work done under this work plan. I strongly suggested
that his client enter into an Administrative Order on Consent (AOC) with the Inactive Hazardous
Sites Branch so that site work is recognized by the state. I also explained that while his Work plan
proposed to perform lagoon closure and soil removal prior to the installation of monitoring wells, it
would be better to install the monitoring wells and sample the groundwater first in order to determine
the level of contamination in the groundwater. This is because the soil cleanup levels are based on
whether or not groundwater is contaminated above MCLs. This would be the most cost effective
means of conducting a cleanup to NC standards.
Mr. Leonhardt informed me that the surface water results had been received and he and Mid-
Atlantic were meeting with Water Quality personnel next week to determine how and where the
lagoon water should be disposed.
Due to my concern over worker safety, I informed Mr. Leonhardt of beads of mercury on a
plywood box at the rear of the building. This box is about chest height and is attached to the rear
comer of the building nearest to the aboveground tanks. Due to its height and location under a cover,
this could serve as a writing surface for onsite workers.
• •
MEMO TO FILE
DATE:
FROM:
NC Superfund
February 4, 2000 9" J_;_ ;/ Ly
Jeanette Stanley, Environmental Chemist, . .,;:;tlit ~()
SUBJECT: Cristex Drum Site
Today, I spoke with Derr Leonhardt, Leonhardt Consulting [phone], consultant
for Cristex Drum. He said that he had just received the PRP letter from EPA regarding the drum
removal and he and Cristex representatives (heirs/ estate holders of Mr. Christiansen) are in the
process ofresponding.
Regarding cleanup of the site, an REC, Mid-Atlantic Assoc. has been retained. Lagoon water
and sludge has been resampled and results are expected soon. They plan to close/remove
above-ground tanks and any contaminated soil underneath these tanks. They also plan to remove
contaminated ditch soil.
For the groundwater study, plan to install several (more than 3) groundwater monitoring wells in
order to conduct a groundwater study. Cristex is under the gun to respond to ]FD/Channel
Master's suit (whether or not Cristex contributed to their GW plume) as well as the issues raised
as a result of the SI.
Mr. Leonhardt expects to receive the sampling/ groundwater study plan from the consultant very
soon, and will forward a copy of this plan to me if! wish to review it or comment on it.
They hope to complete most of this project by this summer.
I told Mr. Leonhardt that we had and ES! on our Work Plan but we may hold off on it for
a while to see how they progress.
• •
MEMO TO FlLE
February 4, 2000 _ _ -~-'J
Jeanette Stanley, Environmental Chemist; w;,
NC Superfund
Cristex Drum Site
DATE:
FROM:
SUBJECT:
Today, I spoke with Derr Leonhardt, Leonhardt Consulting [phone], consultant for
Cristex Drum. He said that he had just received the PRP letter from EPA regarding the drum removal
and he and Cristex representatives (heirs/ estate holders of Mr. Christiansen) are in the process of
responding.
Regarding cleanup of the site, an REC, Mid-Atlantic Assoc. has been retained. Lagoon water
and sludge has been resampled and results are expected soon. They plan to close/remove
above-ground tanks and any contaminated soil underneath these tanks. They also plan to remove
contaminated ditch soil.
For the groundwater study, they plan to install several (more than 3) groundwater monitoring
wells in order to conduct a groundwater study. Cristex is under the gun to respond to JFD/Channel
Master's suit (whether or not Cristex contributed to their GW plume) as well as the issues raised as
a result of the SI.
Mr. Leonhardt expects to receive the sampling / groundwater study plan from the consultant
very soon, and will forward a copy of this plan to me if! wish to review it or comment on it.
They hope to complete most of this project by this summer.
I told Mr. Leonhardt that we had and ES! on our Work Plan but we may hold off on it for a
while to see how they progress.
♦-
. LEONHARDT
ENVIRONMENTAL -·;t ~ .. · ;.~-~
January 22, 1999
State of North Carolina
Division of Waste Management
40 I Oberlin Road
Suite 150
Raleigh, North Carolina 27605
Attention: Donna J. Wilson
Subject: Cristex Site
Oxford, North Carolina
Dear Ms. Wilson:
3208 1\vin Leaf Drive
Raleigh, North Carolina 27613
[phone]
FAX [phone]
RECEIVED
JAN 26 1999
SUPERFUND SECT!()~'
As we have discussed, Mr. George Christensen, owner of the Cristex site, at your request,
suspended all environmentally related activities at his site in Oxford, North Carolina, pending the
completion of your agency's investigation into the possible sources of nearby groundwater
contamination. As we understand it, the portion of your investigation dealing with the Cristex site
has been completed. It is our intention to now resume activities at the site which will include the
closure of the former wastewater treatment lagoon.
We intend to begin the lagoon closure by either removing the sludge remaining in the lagoon, for
disposal off-site, or by chemically fixing the sludge such that disposal on-site can be
accomplished. All activities will be performed in strict accordance with applicable State, Federal,
and local environmental regulations.
If there are any remaining reasons why we cannot begin these activities, please advise us
immediately. We plan to initiate these steps as soon as weather permits, hopefully within the next
90 days.
Thank you for your continuing assistance in this matter. I note that you have advised me that you
will no longer be project manager for this project. I assume that this notification will be
forwarded to your replacement.
Sincerely,
LEONHARDT ENVIRONMENTAL
0_.__:j~
H. Derr Leonhardt II, PE
Consulting Services in
Engineering and the
~-tvironment
• • NORTH CA~OLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WASTE MANAGEMENT
December I 8, 1998
Mr. Tommy Brooks
807 Lewis Street
Oxford, North Carolina
SUBJECT: Well Sampling Results
Cristex Drum Site
N C000 I 606250
Oxford, Granville County, NC
Dear Mr. Brooks:
As you are aware, the NC Superfund Section collected samples from your
drinking water well at 807 Lewis Street on August 13, 1998 as part of an environmental
assessment of the subject site. Samples were analyzed by the State Laboratory of Public
Health for the chemicals listed on the attached sheets. The contaminants listed below
were detected in your well water sample. Concentrations are expressed in parts per
billion (PPB).
Contaminant
Acetone
Carbon disulfide
1, 1 dichlorethane
isopropylether
i=interim standard
Concentration
(PPB)
2.5
0.6
trace
trace
NC Groundwater
Standard (PPB)
700
700(i)
700
70(i)
These contaminants were measured at concentrations which are below applicable
NC Groundwater Standards. No drinking water standards (also known as Maximum
Contaminant Levels (MCLs) considered acceptable for public water supplies)) have been
established for these compounds. These results were reviewed by the State Occupational
and Environmental Epidemiology Section _and they have concluded that your water is
safe for continued usage. A copy of their evaluation is attached for your information.
401 OBERLIN ROAD, SUITE 150, RAI..EIGH, NC 27605
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY/ AF'FJRMATIVE ACTION EMPLOYER· 50% RECYCLED/I 0% P0ST•C0NSUMER PAPER
Mr. Brooks
12-18-98
Page 2
•
If you have any questions regarding health concerns, please contact Dr. Ken
Rudo, Occupational and Environmental Epidemiology Section at [phone]. If you
have any other questions, please contact Jeanette Stanley, Superfund Section at (919)
733-2801, ext. 318.
attachments
cc: Dr. Ken Rudo
File
Donna Keith
Jeanette Stanley
Pat DeRosa, Head
Site Evaluation and Removal Branch
NC Superfund Section
..
i/;lj•; ~l ' ; '
~ti.WAYNE MCDEVITT,~/ ;,.t
1.V.~.'•• .. •".;· y .,_;'1,~~i)jt
~-,;.,.
k .
!~
'
~~~ ~:~~...,--~a tJ,_~'lf~!T -•
;~--.
j,~ ,.
~J:~~~-~~i
·---~:-
~~~~~ ... -:-~{-U ~;,~_.:.,.i:-:• t'.ltM~"n<,.;c•., ~~"" ;~ ll!. ~~, ... ~-:~~
,.·, 'c'I-.
'· {t
f.➔;
• • NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WASTE MANAGEMENT
December I 8, I 998
Mr. Hoffman Suitt
812 Lewis Street
Oxford, North Carolina
SUBJECT:
Dear Mr. Suitt:
Well Sampling Results
Cristex Drum Site
NC0001606250
Oxford, Granville County, NC
As you are aware, the NC Superfund Section collected samples from your
drinking water well at 807 Lewis Street on August 13, 1998 as part of an environmental
assessment of the subject site. Samples were analyzed by the State Laboratory of Public
Health for the chemicals listed on the attached sheets. The contaminants listed below
were detected in your well water sample. Concentrations are expressed in parts per
billion (PPB).
Contaminant
Acetone
Carbon disulfide
I, 1 dichlorethane
isopropylether
i=interim standard
Concentration
(PPB)
2.5
0.6
trace
trace
NC Groundwater
Standard (PPB)
700
700(i)
700
70(i)
These contaminants were measured at concentrations which are below applicable
NC Groundwater Standards. No drinking water standards (also known as Maximum
Contaminant Levels (MCLs) considered acceptable for public water supplies) have been
established for these compounds. These results were reviewed by the State Occupational
and Environmental Epidemiology Section and they have concluded that your water is
safe for continued usage. A copy of their evaluation is attached for your information.
401 OBERLIN ROAD, SUITE 150, RALEIGH, NC 27605
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY/ AF"F"IRMATIVE ACTION EMPLOYER· 50% RECYCLED/I 0% POST-CONSUMER PAPER
Mr. Suitt
12-18-98
Page 2
• •
If you have any questions regarding health concerns, please contact Dr. Ken
Rudo, Occupational and Environmental Epidemiology Section at [phone]. If you
have any other questions, please contact Jeanette Stanley, Superfund Section at (919)
733-280 I, ext. 318.
attachments
cc: Dr. Ken Rudo
File
Donna Keith
Jeanette Stanley
Sincerely,
j)
Pat DeRosa, Head
Site Evaluation and Removal Branch
NC Superfund Section
"
--• •
North Carolina
Department of Health and Human Services
Division of Epidemiology
P.O. Box 2960 I • Raleigh, NC 27626-060 I
James 8. Hunt Jr., Governor
DEC 16 1998
/7-/10/if DA TE ___ __,__,_ _______ :,,-,-,uPERcUMD Si:C:TIQt,'
FROM:
SUBJECT:
Kenneth Rudo. Ph.D .. Toxicologist
Medical Evaluation and Risk Assessment Branch
Occupational and Environmental Epidemiology Section
~ l4i ~fl)c ,?_,"k-:-k:i,
~ixvi llt [~.._~
Attached are the Occupational and Environmental Epidemiology Section's drinking water health-
risk evaluations for the well water samples from the above site. Recommendations for continued
water use are also provided_
If you have any questions, please call me at [phone].
KR/rm
.Vorrh Carolina: Host of:he 1999 Special Olympics World Summer Gumes
. ·-
DATE
()
• •
NORTH CAROLINA DEPARTMENT OF HEALTH AND HUMAN SERVICES
DIVISION OF EPIDEMIOLOGY
OCCUPATIONAL AND ENVIRONMENTAL EPIDEMIOLOGY SECTION
DRINKING WATER HEALTH RISK EVALUATION
GENERAL
COUNTY_~W"--"---'~v~,v_;~//_t __ LABORATORY# '1,f2b/1/ ftz0'.r
{J///z.1
Based of these analytical results, this water should be considered safe for normal usage.
Chemical analysis did not show any contamination. Water should be resampled if odor or taste
persists.
( ) The water should not be used for drinking or cooking purposes; avoid prolonged
bathing/showering.
( ) Bases in these analytical results, this water is highly contaminated and should not be used for
drinking, cooking, or bathing/showering.
() The laboratory results are not conclusive, please resample.
PLEASE INDICATE ON LAB SHEET THAT IT IS A RESAMPLE AND
PROVIDE PREVIOUS SAMPLE NUMBER(S).
COMMENTS:
For further information, contact Dr. Ken Rudo, Occupational and Environmental Epidemiology
Section, [phone].
DHHS 3891 (2/98)
Occupational and Environmental Epidemiology Section (Review 2/01)
// ,, . -. _;;eoi ot tnv1runmcnt, .\{PLE A.l'IALYSIS REQUEST • State Laboratory of Public Hc...1dt,h
P.O. Bo,: 230,17, 306 N. Wilmingwn St. ~ J,. N•wn.l Ruourcc.s
· ~.,1..e /,\ .. a.ofcment D'.-.-i,iu;s; Ralci);h. North Carolina 27611-8047
,;,c Number _,/i/"'-ute.JoCL._!L0-"'O'---'-/ _Jl,ClLo-"'O_ub'-----"'.~-'---"'.5'-----=-0 __ Samp 1e ID N U!I
Name of Site Collected By
C0-032-PW 08/13/98 1308 GRAB
12345678 CD081098, NC D. WILSON
POTABLE WELL
ORG-CLP VOA Ground Waler
Ag::1cy: H=rdous Waste Solid Waste
Sample Type
-Ground Water (1)
Surface Wate, (2)
Environment:11 Concentrate Commenlli
_ Solid (Sf ,_L\f1.l\/c../,~~--~---0J_)v/f,--t
C .
_ Liqui<l (6) ~';[tcJp ~ -
-Soil (3)
-Other (4)
_ Sludge (7) Brooks/ 5u.r'ff
wdt Other (8)
Organic Chemistry Inorganic Chemistr;·
ParillJ)£f'er
-~P&T:CC/MS
Results (mg/!) Parameter Results(mg/l)(mg/kg)
-
Acid: !JIN Ext.
2,4-D
2,4,5-TP(Silvex)
chlo,danc
heptachlor
hexachloroben.l.t!□ e _____ _
hexachlorobut.adiene ~-----
endri.n
lindane
methoxychlor
toxaphene
FOR LAB USE ONLY
Date Received ?--II/--rrvf' (J) G :::,
Date Extracted _________ _
Date Analyzed ~g~·~J=~'--_Cf,_?"-'--o;}~_
Reported By
Date Reported _________ _
Lab Number 98'.ZG1c\
-
-
-···-·
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
antimony
arsenic
barium ------
bef);l!illm
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese
mercury
nickel
nitrate
selenium
silver
sulfates
thallium
vanadium
zinc
pH
conductivity
TDS
flash point
109
TCLP Compound.s
Inorganic CompoWlds Results (mg/I)
arseruc -barium -cadmium -chromium -le:id -
-mercury
selenium -silver -
-
-
-
-
Organic Compow1ds Results(mg/1)
benzene -
carbon tetrachloride -chlordane -· .. --··---,·------...
chloroben.zent! -
chloroform -
o-cresol -
m-cresol -
-p-<:resol
cresoi -I ,4-dichlorobenzene -
1,2-dichloroethane -
-1, 1-dichloroethylene
-2, 4-dichloroethylene
-heptachlor
hexachlorobeazene -hexachlorobutadiene -
~ hexachloroetbanc -
-methyl ethyl ketone
n.itroben:z.ene -
. -pent.achlorophenol
-pyridine
tetrachloroetbylene -
-trichloroethylcne
-2, 4 ,5-trichlorophenol
-2, 4 ,6-trichlorophenol
-vinyl ch.Joride
endrin -
lindane -
-methoxychlor
-toxapbene
2,4-D -
-2,4,5-TP (Silvex)
I
I ;
.ATE LABORATORY OF PUBLIC HEJAH
PO BOX 28047 -306 N. WILMINGTON ST., RALE"'Pl!H. NC 27611
ORGANIC CHEMICAL ANALYSIS
PURGEABLE COMPOUNDS LAB NO 9 'o2lP13 9826/ '+ q924i15 982Co!l.o CJ62h/7
FIELD NO C:P-031-G\.\ cC>-o~~p,.; co-D'f0-5w CD-lbZ-&W co-12-e,,-5w
COMPOUND TYPE ( I ) ( ;i... ) ( ::2. ) ( I ) ( ;;i...)
J, MDL~ ~ ~ 9 (§\ ppm ~ ppm ppm ppm ppb ppm
(nnb)
CHLOROMETHANE ,2. ,0 U-LL I I I J l,L
VI.NTL CHLORIDE J,(p
BROMOMETHANE / J
CHLOROETHANE
TRICHLOROFLUOROMETHANE ' ( ,/ .
1,1-DICHLOROETHENE o.5 I Go. 'i3 ,J ,/ ,l/
ACETONE ;2.,0 3.tf:S,L ;. . 5 :5,c. "J.' '1 -S,C-it.9 :J,L.
IODOMETHANE (),5 I • u._ u..... IA...-
CARBON DISULP'IDE '1-, o.~c.. 0,/J) c..... 0,5 c...
METHYLENE CHLORIDE 5'-1-,R LL / l . I I
ACRYLONITRILE I 1
TRANS-1,2-DICHLOROETHENE
,/ 'I I
METHYL-t-BUTYL-ETHER
1,1-DICHLOROETHANE 0, .-?J ti---ve -J-v-r,re...·
I l f-,r, ce .'/ +,orP !/
ISOPROPYL ETHER
CIS-1,2-DICHLOROETHENE \ I 55.:2_
2-BUTANONE ;2.0 IJ
TETRAHYDROFURAN J.,. ,,-
CHLOROFORM D,5 -/-yf) Ce.
l, l, 1-TRICHLOROETHANE 2,2-
CARBON TETRACHLORIDE lL
BENZENE +vn rP
1,2-DJCfil,OROETHANE LL.
TRICHLOROETHENE 14'7. )_.
1,2-DICHLOROPROPANE u
DIBROMOMETHANE '\ I .J/
C ~ Possible lab contamination or background
J -Estimated value
l,L...
' I
K -Actual value is known to be less than value given.
L -· Actual value is known to be greater than value given.
\ I
+,Aro
J
' I \ /
U -Material was analyzed for but not detected. The number is the Minimum Detection Limit.
NA -Not analyzed.
/ j
--JI
1/ -Tentative identification. b
D -SAMPLE DILUTED. MDL' S DO NOT APPLY. +trO (.(l ; <. C) , 5 pf
qg 2Cot9
CD-100-TB
( '-I )
63 ppm
u_
, I
5,0
I '
\
DHHS 3065-1 (1/98) PURGCOM2.OR
"TATE LABORATORY OF PUBLIC HEALTH
PO BOX 2.7 -306 N. WILMINGTON ST., RAL •• NC 27611
ORGANIC CHEMICAL ANALYSIS
PURGEABLECOMPOUNDS LAB NO qgZ6-i3
FIELD
NO
COi\fPOUND TYPE I I l + MDL}
(~~bl
/~ p~ ppm
BROMODICHLOROMETH.ANE o.5 u._
CIS-1,3-DICHLOROPROPENE
4-METHYL-2-PENTANONE .
TOLUENE
TR.Af.lS-1,3-DICHLOROPROPENE \ I
1.1,2-TRICHLOROETHANE -h"r, C."'
TETRACHLOROETHENE 180,'7
2-HEXANONE u__
DIBROMOCHLOROMETHA.."iE
ETHYLENE DIBROMlDE • I
CHLOROBENll;'IB +(0.C.P,
1, l, 1.2-TETRACHLOROETHA..'iE I I
ETHYL BENZE:iE
XYLE:'iES
STYRENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
1,2,3-TRICHLOROPROPANE
1,4-DICHLOROBENZENE
' I 1,2-DICHLOROBENZENE
J.,O -1.2,-DIBROM0-3-CHLOROPROPANE
C -Possible lab contamination or background.
J -Estimated value
C/62.w I 'f
I ;2..1
8 ppm
LL
'
K Actual value is known to be less than value given.
L -Actual value is known to be greater than value given.
qgzw1!5
I Al
sppm
I I
, I
-h'n rP
I I
./
qg z (jJ) f.t; CJf}Z({J/7
I ) l I Al
8 ppm 8 ppm
I 1 I ,
,/ / ' I ,
-/-,n r P J/ +-y-o,,., Y
+rnrP +v-r, Cf'
J I I
,/ . /
+,C,rP-: +,-ace.!.
I , I I
.
I I ·, .
U -Material was analyzed for but not detected. The number is the Minimum Detection Limit.
NA -Not analyzed.
1/ -Tentative identification.
D -SAMPLE DILUTED. MDL'S 00 NOT APPLY.
DHHS 3065-2 (1/98l
q82c,, 18
( '1)
eppm
LL..
\ I
PURGCOM2.0RG
• · c LJcpa;"":.:nent of En·,ironrnen:,
He.allh, & N.1.rural Ruource,
5olid Wut.c M.a.n.agcmcn\ Divi,ion
SAlvlJ'LE ANALYSIS RF.QUEST Sute. Laboratory of Public Hc..ah.h
P.O. Bo:t :!8047, 306 N. Wilmington St.
Ra!ci1;h, North Carolina 27611-8047
Si le Number ___J/0c.:...LCuD:.L-.-"'0'-'D'°-,f,__j_Jfe"-"'D-1(-"o-?~"-z;:-,_,._C'...,,c... Sarnp le ID N UJ C0-031-PW 08 / 13/98 1308 GRAB
. _J_ 12345678 CD081098, NC D. WILSON
C,(<,fl'Y rDo, fr) ,S:zi= ,Collected By. POTABLE WELL
tf\ j) J ORG-CLP EXT/PCB Ground Water
V '/ 17/)7 fl}(.__ DatcCollecl«. __
Name of Site
SiteLoc:i.tion -
Agency: H=irdous Waste Solid Waste ~fund TCLP Compounds ----
111
Sample Type Inorganic Compounds Results(mg/1)
Environ.men la I Concentrate Comments -arsenic
. ✓Ground Water (1)
-barium
Solid (5) cadmium --chromium -
Surface Water (2) Liquid (6) lead ---
-mercury
-Soil (3) Sludge (7) -selenium -silver -
-Other (4) -Other (8) -
-
-
Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Par::irneter Resul ts(mg/l)(mg/kg) Organic Compounds Results(mg/1)
~T:GC/MS -antimony benzene ---
_ 1d:B/N Ext. arsen.ic carbon tetrachloride --
-2,4-D -·-barium ·---chlorc!E.ne ·---------·--·· ----·-·---···-·-·--·----·
-2,'i,5-TP(Silvex) -beryllium -chlorobenzene
chlordane -cadmium ·-chloroform -he;::tachlor -chloride -o-creso! -
-hexachl oro benze:J e -chromium -m-cresol
-hexachlorobutadiene -cobalt -p-cresol
-endrin -copper -cresol
-lindane -fluoride 1,4-dich!orobenzene -
-rnethoxychlor -iron -1,2-dichloroethane
-toxaphene -lead I, 1-dichloroethylene -
.JL'"" £.C. B. :i <O.{)OO<~n,._ -manganese -2, 4-dichloroetbylene
--mercury -hepta.chlor
nickel hexachJorobenzene ---
nitrate bexachlorobutadiene ---selenium ~ bexach.loroethane --
-silver methyl ethyl ketone -FOR LAB USE ONLY -sulfates nitroben.z.ene -
-thallium pentachl orophenol
Date Received g'-Jt/~jfldG -vanadium pyridine --RB~ 'i'-/3-9?'-vP · -zinc tetrachloroethy lene -
Dale Extracted {llJ {t<(--f7-9s,' /.!~;;wl r -pH trichJoroethy lcoe -6/Jlf ",7 g'..f t3 . -conductivity -2, 4,5-trichlorophenol
Dace Analyzed P@:s g:..,;;7, tJ-~VP -TDS 2, 4, 6-trichlorophenol -
-fla.sh point -vinyl chloride
Reported By --endrin
!ind.me --
Date Reported --methoxycWor
982595 --toxaphene
Llb Number 2,4-D --
--2,4,5-TP (Silvex) ..
• STATE LAW'J\TOHY Of P\JBLIC HEALTH • P.O. 2,0X 28047 -3% IL lllLHlNGTON, ST._ RALEIGH, N.C. 276)1
ORGANIC D1EMICAL ANALYSIS
BASE/NEUTRAL AND ACID LAB NO ,QVc:J_--,q,f iO.,, r:<1, cxi-, ,,-q/,.. t/Y2 <:c77 Ov'1~Y
EXTRACT ABLES FIELD # "l)-o3i,r;..,, ".0-,,,:2-,_pw a~ -""O • 0 ,J f'l\-11;;> -r.:.·w "'1}-/ >/.-lw
COMPOUND TYPE I I ) I J ) ( ;z) ' I l (~)
UNITS /"0111,-.. "n/ 1' --~ ,, n / J '1.-m-+.. n .. n/]~ uQ/1 )...-,
.~-n 1 trosodirrethvl amine IOI -'~O ., -•, -. -,( ~ , A· -i L-
bis(2 chloroethv])ether
2 chlornnher:cl
ohenol
l 3-dichlorobenzene
l.4-dichlorobenzene
l 2-<Jichlorobenzene
bis(2-ehloroisnnrnn"J)ether
hexachloroethane
N-nitroso-di-n ~r....,..."lamine
nitrobenzene
i S""horone
2-ni trnnhenol
2 4-<Jirrethv]ohenol
bis(2-ehloroethoxv)rrethane
2.4-<Jichlornnhenol
1 2 4 trichlorobenzene
nanhthalene
hexachlorobutadiene
4-chloro-m--cresol
hexachlorocvcl~ntadiene
2 4 6 trichlornnhenol
2-chloronanhthalene
acena0 hthvl ene
dirrethv] nhthalate
2 6-<Jinitrotoluene
acenanhthene I
2 4-<Jinitrnnhenol SOh<t,SO
2 4-<Jinitrotoluene 107:r-=io
4 nitrMhenol ""01,,_.:o
fl uorene 107330
4 chlornnhenvJnhenvlether
diethvl nhthalate -,
4 6-<Jinitro-o-cresol r,;_ <"O 50 1
dinhenvlamine /0 1 330
azobenzene
4-br~henvl nherivlether
hexachlorobenzene
,,,
=ntachlornnhenol sol11.:ro
nhenanthrene ,,,, / ~~{)
anthracene
dibutvl nhthalate I I/ I/ I I
fl uoranthene ,., I I I ' ~
J -Estimated value_
K -Actual value is known to be less than value given.
L -Actual value is known to be greater than value given.
U -Material was analyzed for but not detected. The nurber
NA -Not analyzed.
is the ~inirrun_Qetection !:_imit. m'J:JL -
l/ -Tentative identification. £1 -On NRDC List of Priority Pollutants.
tlx',;I\']Cj
11TJ-.)00-1<A
( 4)
.. n/)~q
vL--
I/
'
• STATE LABORATORY Of l'UBLlC IIEAL1.
P.O. BOX 28047 -306 H. \/lLHlNGTON, ST., RALUGH, N.C. 2761 !
OOGNHC CHEHlCJ\L ANAL YS 1S
BASE./HEUTRAL ANO AClO LAB NO I t/'x' .:J.:5 <-IL/ i'1li",)"i.,, \ :CJ ,f' .2. ,;91,, '-IX,:J \'-f7 i'IV?("'}y
EXTRACTABLES FIELD # [('j).03/-G,1, ~'1>. ,.n .A, ; ('r,-c)(jh-x,_) r:JJ-113viw ('1)-i,){,~<.·, l
COMPOJNO TYPE ( J ) ( I ) (.A ( ) ( .2. l
UNITS uo/1 l__,t..-u0/1 \.~ii.~ u a/ 1 I """"" un/ 1 " ua/1 "
'
nvrene JO/ i:io I.L -I -\IL--L-~
benzidine ,nl '"50 I
butv1 benzv1 ohtha1ate JO/ '130
benz(a)anthracene
chrvsene .
3 3-<1ich1orooenzidine it.So SO/
bis (2-ethv1 hexy1 )phtha 1 ate I0/330
di-n-octv1 ohtha1ate /0/3-?o
benzo(b)fluoranthene so/1.,So
benzo(k)fluoranthene
benzo (a lnvrene
i ndeno ( 1 , 2 3--ed l nvrene
dibenzo(a h)anthracene / / ,. / /
benzo(a h i 10<'ry1ene \,. ' ' I ' ' I \
aniline <o 1,1,,,.-0 I -t IA ):, -IA--
benzoic acid
benzvl a lcoho 1
4--eh 1 oroan i 1 i ne ' .,,
dibenzofuran 10 IZ-10
2-<rethvl n>nhtha 1 ene
2-methvl oheno 1
4-methvlphenol ~,
2-nitroani 1 ine S'o ·, t,,5o
3-nitroani line
4-nitroaniline / I I / /
2,4 5-trichloroohenol
,_:, \ \ \ ~ ' I
f)'J 1) L-
J -Estimated value. H.:. O I Soll.
to be less than value given.
to be greater than value given. K -Actual value is known
l -Actual value ls kno.t'n
U -Katerla1 was analyzed
NA -Not analyzed.
for but not detected. The nmber 1s the MinirruT1 Detection Limit.
1/ -Tentative identification.
~/ -On HROC List af Priority Pollutants.
,9!? ..).,\'/Cj
1"7>-1, C7I -E' /:!.
( '.fl
ua/1 "
V
'
I~ -
/
'
NC Dep1nmenl of E:wiror.mc.nt,
Hu.Ith,&. N,wn.l Ruource,
Solid Wu1.e Marugcmc.nl Divi,ion
.,Vvil'LE Ai'IALYSIS REQUEST • Sute Labor11l0ry of Public Hu.1th
P.O. Box; ~8047, 306 N. Wilmington St.
R,leibh, Nonh C.aroli..n, 27611·8047
Site Number _/0'-"-'(!,,"':..;0"-'C)"-'0"'-'/~(o~Q~LJ~(l~J.ac.,..,_D_'V~--Sample ID Number,
Name of Site Cridrx Dcu 01 5,·fe.----CoIIec,edBy_·_.
'
CD-032-PW 08/13/98. l308 GRAB
l1345678 CD08!098, HC D. W!LSOH
POTABLE WELL.
!HORG-CLP METALS Ground Water
112 Si le Loc;i tion _,_Q,,___x,._,_fo..u...,_c,.,_0"'~~-"";J.,_.,.0"'''----Date Callee tro
Agency: Hazardous Waste Solid Waste _0uperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentr.:ite Comments arseruc -barium -Ground Water (I) Solid (5) cadmium ---chromium -Surface Water (2) Liquid (6) -lead --
-mercury
Soil (3) Sludge (7) selenium ---silver -
-Other (4) -Other (8) -
-.
-Organic Chemistry Inorganic Chemistry ,
-~
Parameter . Results (mg/I) ~eter Results(mg/1),W,II • Organ.ic Compounds Results(mg/1)
-P&T:GC/MS antimony .,_o _,,, o& benzene -
-Acid:B/N Ext. _J,..---"f Se n.i C 4-Q-o l carbon tetrachloride -
-2,4-I: _.i,..)>irrium <'.. 0 -l -----. -·-chlordane
-2,4,5-TP(Silvn) _ beryllium -chlorobenzene
chlonl.".ne ~ mi Um '--0-005 chloroform --
-bept.a1;Wor chloride o-cresol --
-hexac~!lorobemene ~omiurn L.o,ol m-cresol -
-hexachlorobut.adie□e cobalt p-cresol
ppper -endri.n L..o.a5 cresol --
-lindane fluoride 1,4-dichlorobenze□ e --
-methoxychlor iron 1,2-<lichloroethane --
-toxii.phene ~ad ~o.c,o5 -1, 1-dichloroethylene
--ITL1nganese -2, 4-dich!oroethylene
-~ercury zo .cs:ia5 -heptachlor
-~ckel 4-C, -l':) 1 -bexachloroben.zcne
nitrate hexachlorobutadiene -
~enium
-L_a .ca,:5 ~ bexachloroetbane -
~ver "'-D-c.5 -methyl ethyl ketone
FOR LAB USE ONLY Sulfates nitrobenzene --thallium pentachlorophenol --Date Recei·,., :.d vanadium pyridine --~inc L_ 0-o5 -tetraChlor·Oethylene
Date Extracted pH trichJoroethylene --
-conductivity -2, 4,5-trichloropheno]
Dale Analyzed -TDS 2,4,6-trichlorophenol -
-flash point -vinyl chloride
Reported By ··--endrin
. lindane --
Date Rcrrr1-2s AUG 1798 --methoxychlor
toxaphene --Lab Number 2,4-D --
--2,4,5-TP (Si!vex)
OHS·) !9! {R.:vi~~d 11/93)
• • NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WASTE MANAGEMENT
November 25, 1998
MEMORANDUM
TO: Dr. Ken Rudo, Toxicologist
Occupational and Environmental Epidemiology Section
THROUGH: Jack Butler, Chief~
Superfund Section
FROM: Pat DeRosa, Site Evaluation and Removal Branch Head {¾,cl,.l("-
Superfund Section
SUBJECT: Health Risk Evaluation Request
Cristex Drum Site, NCO 001 606 250
Oxford, Granville County, NC
Please find attached a copy of the laboratory analyses for a well sample
collected by the Superfund Section near the subject site. Since this sample was
collected from a drinking water well, the Superfund Section requests a health risk
evaluation and a recommendation on the continued use of the well. This
information will be provided to the affected well user. If you have any questions
regarding this matter, please contact Donna Wilson or me at 733-2801.
attachments
cc: File
Donna Keith
Donna Wilson
PD/EPIJ
401 OBERLIN ROAD, SUITE ISO, RALEIGH, NC 27605
PHONE[phone] FAX [phone]
AN EQUAL OPPORTUNITY/ AFFIRMATIVE ACTION EMPLOYER -50% RECYCLED/10% POST-CONSUMER PAPER
/ /',:ni 01 .t.nv1ronmc:nt, .vIPLE A1'-IALYSIS REQlJEST • Sui.tc Laboratory of Public He.al1.h
P.O. Box '.::3047, 306 N. Wilmin_g1on S1. ~ & N1rur.1I Ruourccs
-i,\/Ht.e Ma11-1i;:cment Di,,i,ion
,,,d'iurnber ~/J~C-~O~=O~O~/~/o~0~6~fl_CX~--~~D __ Sample ID Nu!I
Name of Site l 1r-i'2fcx Drum ,S>ie, Collected By_
Ralcii;:h. North C,rolin1 2761 J-ao,n
C0-032-PW 08/13/98 1308 GRAB
12345678 CD081098, NC D. WJL50N
POT ABLE WELL
ORG-CLP VOA Ground Waler
109 SiteLoc.11io□ /) X /!o,-r/ , /II L--DateCollecte<l
--,,/.x,__-,,,'-+--~~--/~L~~-------;::======-__:======-,
Age:::icy: Hazardous Wa.ste
Sample Type
Environmental
-Ground Water(])
-Surface Wate, (2)
-Soil (3)
-Other (4) Other (8)
Organic Chemistry
Par~er
VP&T:CC/MS
Results (mg,'!)
Solid Wa.ste
lnorganic Chemistry
Parameter Results (mg/l)(mg/kg)
-antimony
arseruc -barium
TCLP Compounds
lnor<sanic Compowids
a,.--seruc -barium -
cadmium -
chromium -lead -
-mercury
selenium -silver -
Organic CompowHis
beru:.ene
carbon tetrachloride
chlordane
Result.s(mg/1)
Results(mg/1)
I
I Acid:DiN Ext.
2,4-D •.
2,4,5-Tl'(Silvex)
chlordane
bept.acrJor
--·-· ----·-··------------· '.
hexachloroben.ze:Je _____ _
hexachloro butadieoe -------
-endrin
lindane
methoxycliJor
toxaphc:ne
FOR LAB USE ONLY
Date Received 7--/lf-f?'V/; {U G ;,
Date Extracted ----------
Date Analyzed 8'-J'is'-9' f W
Reported By
Date Reported _________ _
Lab Number 982G1<\
DHS 319! (Revised 12193)
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
beryllium
cadmium
chloride
chromium
cobalt
copper
fluoride
iron
lead
manganese
mercury
nickel
n.i trate
selenium
silver
sulfates
thallium
vanadium
ZlllC
pH
conductivity
TDS
flash point
chlorobenzen~ -
chloroform -
o-cresol -
m-cresol -
-p-cresol
cresol -
-1,4-dichlorobenzene
1,2--dichloroethane -
-I, 1-dichloroethylene
-2, 4-dichloroelbyle□ e
-bept.achlor
bexachlorobenzene -bexachlorobutadiene
... bexachloroethane -_ methyl ethyl ketone
nitrobenz.ene -
-pentachloropbenol
-pyridine
-tetrachloroethylene
-tri.chloroethylene
-2, 4 ,5-trichlorophenol
-2, 4, 6-trichlorophenol
-vinyl chloride
endrin -lindane -
-methoxychlor
-toxaphene
2,4-D -
-2,4,5-Tl' (Silvex)
s1TE LABORATORY OF PUBLIC ~I
PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH, NC 27611
ORGANIC CHEMICAL ANALYSIS
PURGEABLECOMPOUNDS LAB NO C\S2wl3
FIELD NO C-P-031-~
COMPOUND TYPE ( I )
~ MDL ,r r, ppm
(nnb)
CHLOROMETHANE ,2,0 U-
VINYL CHLORIDE ;,{p
BROMOMETHANE I •
CHLOROETHANE
TRICHLOROP'LUOROMETHANE '-I ,/
l, 1-DICHLOROETHENE o.5 (G,, 8
ACETONE ;z,o 2}.8-:S,L
JODOMETH.ANE (),5 , ... _
CARBON DISULFIDE }
METHYLENE CHLORIDE Si..\-,~
ACRYLONITRILE I '
TRANS-1,2-DICHLOROETHENE
METHYL-t·BUTYL-ETHER
,/
1,1-DIClll.OROETHANE l..r, :?J
ISOPROPYL ETHER I J
CIS-1,2-DICHLOROETHENE \ I 55,;z_
2-BlITANONE ;2.0 I
TETRAHYDROFURAN J,. \/
CHLOROFORM D,5 +vnc.e...
l, l, 1-TRICHLOROETHANE ,2. 2-
CARBON TETRACHLORIDE lL
BENZENE +r'rt l'P.
1,2-DICHLOROETHANE LL
TRICHLOROETHENE 14'7. ;l.
l,2·DICHLOROPROPANE fl
DIBROMOMETHANE ' I -v
C -Possible lab co.ntamination or background
J -Estimated value
Ci92&t+
cC>-o~-p-,./
( ,;)_J
~ ppm
u_
' I
;. . 5 -:,,c
u._
0, lD c..
( l
,(
+eve
y t-rrl c.e
u__..
I
K -Actual value is known to be less than value given.
L --Actual value is known to be greater than value given.
Q62i.ol5
cD-Ufo-5W
( 2 )
~ ppm
I I
,/
').' '7 J ,c...
L,L.
0, /.J) C_.
/ I
' I
982(.PJ/.,:, !Cl6 z(p r1
CD-ib2-&W C0-/2<,.-5W
( I ) ( ;;i...)
c@ ppm ~ ppm
' J lL
,l/
J.j-, 9 3,c...
LL
0,5 c...
'
• I
}.,.-n.re.. ·
+r-orP Y
I J
\ I
+.-l'lrP
1
·, / -w
U -Material was analyzed for but not detected. The number is the Minimum Detection Limit.
NA -Not analyzed.
1/ -Tentative identification. b
D -SAMPLE DILUTED. MDL' S DO NOT APPLY• +t~o Ce = <. 0 , 5 pp
qg 2(p/ 8
CD-100-TB
( '-I )
~ ppm
u__
' (
.5,0
I ,
' /
DHHS 3065-1 (1/98) PURGCOM2.OR,
A\TE LABORATORY OF PUBLIC ~H
PO BOX 2s!!f'7 -306 N. WILMINGTON ST., RALE •. NC 27611
ORGANIC CHEMICAL ANALYSIS
PURGEABLECOMPOUNDS LAB NO C/SZG->13
FIELD
NO
COMPOUND TYPE I I )
,t MDL ..
(nnb] /i'."'~ ppm
BROMODJCHLOROMETHANE o.5 LL
CIS-1. 3•DICHLOROPROPENE
4-MITHYL-2-PENTANONE
TOLUENE
TRANS•l,3-DJCHLOROPROPENE ,I
1,1,2-TRJCHLOROETHANE -+,r,-,cp
TETRACHLOROETHErn: 90,'7
2-HEXANONE LL.
DIBROMOCHLOROMETHANE
ETHYLENE DIBROMlDE I
CHLOROBENZEN"E +vac.P _
1, 1, 1,2-TETRACHLOROETHANE f I
ETHYL BENZENE
XYLENES
STYRENE
BROMOFORM
1,1,2,2-TETRACHLOROETH.ANE
1,2,3-TRICHLOROPROPANB
1,4-DICHLOROBENZENE
l,2-DICHLOROBENZENE ' I
1,2,-DIBROM0-3-CHLOROPROPANE J,O '
C -Possible lab contamination or background.
J -Estimated value
CJ62(o ! 'f
I Al
~ ppm
CL ,
' I
K -Actual value is known to be less than value given.
L -Actual value is known to be greater than value given.
qf3201.'5
I ;2.. )
sppm
I I
' /
-h'()rP
I I
' I
qgz{,)J~ 9£3Z(pJ7
I ) ) I Al
8 ppm e ppm
I , ( I ., / ' I,
--/-,n ra l/ --h--arP y
+("(l rP +v-r,cP
J I I
' I/ ' /
+rc:trP.!,, +,--cue-'-
I ' I J
-, I I .
U -Material was analyzed for but not detected. The number
NA -Not analyzed. is the Minimum Detection Limit.
11 -Tentative identification.
D -SAMPLE DILUTED. MDL'S DO NOT APPLY.
DHHS 3065-2 (1/98)
q82-IJll8
I '-I )
@ppm
u_.
' /
PURGCOM2.0RG
.: ocpa:1:rn::nt oi E:wironmc:nt,
Hul.h, &. N•OJral Ruourcc:1
Solid Wut.c: Muu~cmcm Divi,ion
SA1vll'LE ANALYSIS REQUEST Su.tc Laboratory of Public Hu.Ith
P.O. Box 28047, 306 N. Wilmington St.
Raleii;h, North Carolina 27611-8047
SiLcNumber /v(;v Oo (
NameofSite C,fsfl'y
fp l) (o « s:::n Sample ID Nu, C0-031-PW 08/13/98 1308 GRAB
11345678 CD081098, NC D. WILSON
SiteLoution e Y &«0 rDcu hi ,5;6;, ,uille<:ted By. POTABLE WELL .
ORG-CLP EXT /PCB Ground Water /} i /' f.J!_ L-----Dale Coil e<:Le<. __ _ 111 -
Agency: --Hazardous Waste Solid Waste ~fund TCLP Compounds --
Sample Type Inorganic Compounds ResuJt.s(mg/1)
EnvironmenL1l Concentrate Comments -arsewc
✓Ground Water (1)
-barium
Solid (5) -cadmium. -chromium -Surface Water (2) Liquid (6) lead ---
-mercury
Soil (3) Sludge (7) selenium ---silver -
-Other (4) Other (8) . --
-
-Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Parameter ResuJt.s(mg/l)(mg/kg) Organic Compounds Result.s(mg/1)
/4T:GC/MS antimony -benzene -
_ 1d:B/N Ext. arseruc carbon tetrachloride --2,4-D barium .. ·---chlordane --· -·---------·--·· -·-
-2,4,5-TP(Silvex) -beryllium -chJorobenzcne
chlordane cadmium chloroform ---
beptachlor chloride -o-cresol --
hexachlorobeaz.ene chromium m-cresol ---
hexachlorobutadiene cobalt p-cresol ---
endri.n copper cresol ---
lindane fluoride -1,4-dichlorobenze□e --
-methoxychJor iron -1,2-dichloroethane -
toxaphene lead 1, 1-dicWoroethylene ---
_Le" e. c. B :i <0.(}00/~ -manganese -2, 4-d_ichloroelhyle□e
--mercury -heptacWor
nickel hexach1orobcnzene· · ---
nitrate bexachlorobutadiene ---selenium ~ hexachloroetbane --
-silver methyl ethyl ketone -
FOR LAB USE ONLY sulfates nitroben2ene --tha.llium pent.achlorophenol
Date Re,:eived ~-Jt;.,--g:rg_-ws --
-vanadium pyridine -zinc tetrach1oroetby Jene RBs 'i'-/3-9 VP --
Date Extracted /jl,!ii_'{_-£1-')_f/l-lrr -pH -trichloroethylene
&JI} '?7 K~ 8 . -conductivity -2, 4, 5-Lrichlorophenol
Date Analyzed eMs F--..:l o-97VP -TDS 2, 4, 6-trichlorophenol -
-flash point -vinyl ch1oride
Reported By --e.ndrin
lindane --Date Reported --methoxychlor
982595 --toxaphene
Lib Number 2,4-D --
--2,4,5-TP (Silvcx)
,-,.,. ' : . ,. ' ' -':.
.STATE LAIJOHATORY Of PUBLIC HEALTH • P.O. llOX 28047 -306 N. \o/lLM!NGTON, ST .. RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
BASE/NEUTRAL AND ACID LAB NO
EXTRACT ABLES FIELD#
COMPOUND TYPE
UNITS
N nitrosodimethvlamine IO/ -<"lO
bis(Z-chloroethvllether
2-chloroohei:sl
ohenol
l. 3-dichlorobenzene
1 4-dichlorobenzene
1. 2-di ch lorobenzene
bis(Z-chloroisooroovl)ether
hexachloroethane
N-nitroso-dl-n-nroovlamine
nitrobeni.ene
i soohorone
2 nitrfV'lhenol
2.4-dimethvlohenol
bis(Z-chloroethoxv)methane
2 4-dichloroohenol
1,2.4-trichlorobenzene
naohthalene
hexachlorobutadiene
4-chloro-m-cresol
hexachlorocvclf'Y"'>t>ntadiene -
2,4,6-trichlornnhenol
2-chloronaohthalene
acenaoh thvl ene
dimethyl nhthalate
2.6-dlnitrotoluene
acenaohthene
2.4-dinitrnnhenol S01 ~hSO
2.4-dinitrotoluene 10 330
4-nitrrv-.henol s-0111~<:o
fl uorene /0/.330
4-chloroohenvlohenvlether
diethvl ohthalate ',
4,6-dinitro-o-cresol 50 '11,,0
diohenvlamine /0/330
azobenzene
4-brcm::,phenvloherivlether
hexachlorobenzene ~
n<>ntachlornnhenol so//<ii5'o
ohenanthrene i,,-,/~-~o
anthracene
dibutvl ohthalate
fl uoranthene ,,
J -Estimated value.
nYDL
H,.o/so1L-
;'-'f\/ . .,._,;u uo,...,,.,,
"'JJ-,J3 i-r,, 1,1,, ,,,~_,,:v-/Jw
< I l ( I l
0q/l I,-., uoll' ..
t,( -11l-
I /
\ '
K -Actual value is known to be less than value given.
l. -Actua~ value is known to be greater than value glven.
C/ 0 ') <;:Cf(,,, 'f X :,,J, "1'/ 7
"1if-/><Jo-<-;, "l)-1 I 1-r;;w
(~) r / l
uo/) l!'mr.wn "n I l hm!l-o
I ;t ~ ,,<
I /
' '
OC-'2rfY
171)-1 v--sw
{.;l )
ua/ l }m-t>,n
I. -
I
'
U -Material was analyzed for but not detected. The nurber
NA -Not analyzed.
1s the Minirrun Detection Limit. mIJL ---
l/ -Tentative identification.
fl -On NROC List of Priority Pollutants.
'fl( c7, \ "/'1
"7>-.2oO-l?,t;!
( i/)
uo/ l'rm,llco
vL--
/
'
BASE/NEUTRAL AND ACID
EXTRACTABLES
COMPOOND
rwrene
benzidine
butvl benzvl ohthalate
benz(a)anthracene
chrvsene
3 3-<lichlorobenzidine
bis(2-<ethvlhexvl)phthalate
di-n--octvl ohthalate
benzo(blfluoranthene
benzo(k)fluoranthene
benzo(a) ovrene
i ndeno ( l 2. 3-cd) ovrene
dibenzo(a h)anthracene
benzo(o h il=rvlene
aniline
benzoic add
benzvl alcohol
4-chloroaniline
di benzofuran
2-methvl naohtha lene
2-methvlphenol
4-methvloheool
2-nitroaniline
3-nitroaniline
4-nitroaniline
2.4 5-trichloroohenol
J -Estimated value.
• STATE LABOfl/'10fn OF l'\JBL!C IIEMlf.
P.O. BOX 28017 -306 N. ll!LMINGTON, Sl., PALElGH, N.C. 21611
OOGANIC Qj£MICAL ANALYSIS
LAB HO qy ,)_', 1 <I 199.J ,:;q 1 .a P1.S"/t,, q5i'...1 '\Y 7
FIELD # C'il-ll3/-G,t, ~'ll-,,;,.;, -A, l'n-v<lt, -:J,,J ('_j}-113-Giw
TYPE i I l i I ) (_.}.J ( )
UNITS uo/1 )..,.J.w, uq/1 \.,..,~ " o / I \.,,.,,..., v;,o/ l) ,,
10/:1::io LI.~ I -v<---
. '.11 l1t,SO ,.
101_:130
. ,
sa/tb5o '
10/330
/0/3-~o
SO/Jl:50
t / / /
' / I \ I ' ' I
<'o ,,. \( L -I I IA -
' r
101=0
~:,
S'o/,t,,5o
/ I I /
\/ ' \ \
-
/')') 1) 1-
Hz O / Soll-
to be less than value given.
'-/VJ\ '19
('1)-iX.~<.:,)
( ? )
,,.-uo/ 1'
,l -
/
\
vL-
/
K -Actual value is known
L -Actual value is known
U -Katerial was analyzed
NA -Not analyzed.
to be greater than value glven.
for but not detected. The nurber is the HinilTUT! Detection Limit. m:zn .. -
1/ -Tentative ic1entification.
2/ -On NROC List of Priorlty Pollutants.
-~ ,,,
r_J)-1., r,, -e /?,
( './-)
uo/1 "
' • -
,
'
LI -
/
'
NC Dqartment oi E:wirorunent,
Hu.Ith,&. N.rn.1nl Ruourc:c,
Solid Wu~ Man.a~ement Divi,ion
.\1\1:PLE Al'iALYSIS REQlJEST • SL.ate Laboratory of Public: Health
P.O. Box 18047, 306 N. Wilmington St.
Raleibh, North C1roli.n1 27611-8047
Sit,: Number ~M'--"--'t""'--'0"--'C?"-'O""----'/--"'(oc..,.O~u~o~2~,..,_<_1J~--Sample rn Number,
Name of Sit,:; Cci 51:< x Dev 01 S , ·f e.----: Collected By_·_.
IJ /) /Aj /v
C0-032-PW 08/13/98 1308 GRAB
12345678 C0081098, HC 0. WILSON
POTABLE WELL
!NORG-CLP METALS Ground Waler
-
112 SiteLoc.:itio□ ~~><-t12~~C~(~)-+~,,-U---~~----Dat,:; Collected
Agency: HW!rdous Wa.st,:; Solid Wa.su: l:c::'.:'su perfun d TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environment.a.I Concentrate Comments arseruc -barium -
Ground Water (l) Solid (5) cadmium ---
chromium -
Surface Water (2) Liquid (6) -lead --
-mercury
Soil (3) Sludge (7) selenium ---
silver --Other (4) -Other (8) -
-.
-
Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) ~eter Results(mg/1; $ .. Organic Compounds Results(mg/1)
-P&T:GC/MS anttmony -Zo .co& -benzene
-Acid:B/N Ext. -L.,--"1 seni c 4.Q. o 1 -carbon tetrachloride
-2,4-I: -.J_..),cium .z_,::, -1 ______ . ----chlordane
-2,4,5-TP(Silvex) _ beryllium -cWoroben.zene
-chlordnne ~ mi U ID .ZQ.,;205 -chloroform
-heptal:Wor chloride -o•cresol -
-hexachlorobe:u.ene ~omi urn L.Q~ol -m-cresol
-hexachlorobutadiene cobalt p-<:resol
~pper
-
-endrin L..o.c;;5 cresol -
-lindane fluoride 1,4-dichlorobenzene --
-methoxychlor iron -1,2-<lichloroethane -
-tox3pbene ~ad :,;c.coS -1, I-dichloroethyle□e
--manganese . -2, 4-dichloroethylene
-~ercur; L..c. <>s:io5 -heptachlor
-~eke] L..c,.c,1 -hexachloroben.zene
n.itrate hexachlorobutadiene -
~elllurn
-
L._<:3 .co-5 ~ hexachloroethane . -
~ver <-o.c.5 -methyl ethyl ketone
FOR LAB USE ONLY sulfates nitroben.z.ene --thallium pentachlorophenol --Date Recc:iv:.d vanadium pyridine --~inc L... 0-o5 -tetraChloiOethylene
Date Extracted pH trichloroethylene --
-conductivity -2, 4,5-trichlorophenol
Date Analyzed -TDS 2, 4, 6-trichlorophenol -
-/la,h point -vinyl chloride
Reported By -endrin ·-lindane --
Date Rarf.t2s AUG 1798 --methoxychlor
t6xaphene --
Lab Number 2,4-D --
--2,4,5-TP (Silvex)
DHS 3191 (Revi~cd 1:2/93)
REMEDIA~TE ASSESSMENT DECISION -E. REGION IV Page 1 of 1
EPA ID: NC0001606250 Site Name: CRISTEX DRUM SITE
Alias Site Names:
City: OXFORD
Refer to Report Dated: 06/30/1999
Report Developed by: STATE
DECISION:
County or Parish: GRANVILLE
Report Type: SITE INSPECTION 001
[ 1. Further Remedial Site Assessment under CERCLA (Superfund) is not required
because:
[ 1a. Site does not qualify for further remedial site assessment under CERCLA
· (No Further Remedial Action Planned -NFRAP)
[ 1 b. Site may qualify for action, but is deferred to:
!5( 2. Further Assessment Needed Under CERCLA:
2a. Priority: [ Higher p( Lower
2b. Other: (recommended action) Low
DISCUSSION/RATIONALE:
Combined PA/SI
Further Action Recommended
Site Decision Made by: KEN MALLARY
Signature:
EPA Form# 9100-3
I I
State ID:
State: NC
Date: 09/30/1999
0
SITE HEALTH AND SAFETY PLAN
A. Genera1 Information
•
Site Name Cristex ID# NCO 001 606 250
Location Corner of Industrial Dr. and Pine Tree
Rd. Oxford, Granville County, NC
Proposed Date of Investigation August 10-14, 1998
Date of Briefing _A_u~g~u=s~t_4~,'--~1~9~9~8~---------------
Date of Debriefing A~u~g~u~s~t----'1~7~,'--~1~9~9~8~-------------
Nature of Visit (check one): On-Site Reconnaissance
Off-Site Reconnaissance
Sampling
Sampling Overview
Remediation Overview
Health Department Official Contacted Mr. Mitchell Arnold
X
X
Date of Contact _J_u_l~_2_7~,_1_9_9_8 _______________________ _
Site Investigation Team: All site personnel have read the Site Health and
Safety Plan and are familiar with its provisions.
Personnel Responsibilities Signature
Team 1 Donna Wilson team leader
Team 1 David Mattison removal evaluation
Team 2 Harry Zinn little beaver
Team 2 Doug Rumford little beaver
Team 3 Jeanette Stanley sampling
Team 3 Doug Moore sampling
Team 3 Stuart Parker sampling
•
B. SITE/WASTE CHARACTERISTICS
Waste Type(s) __ X_Liquid X Solid Sludge
Characteristics Corrosive X Ignitable
Gas __ X_Vapor
Radioactive
X Volatile X Toxic Reactive Other
List Known or Suspected Hazards (physical, chemical biological or
radioactive) on Site and their toxicological effects.
chemical amounts
HAZARD
Tetrachloroethene
Toluene
X lene
Barium
Chromium
Lead
Methylene Chloride
Ethylbenzene
Trichloroethylene
WARNING PROPERTIES
Odor Threshold (OT) = 4.68
OT 0.17 40 eem
OT 0.05 200 EErn
OT no data
OT no data
OT no data
OT=25-30 eem (can ada2t to
OT 0.25 -200 eem
OT 0.2 -400 eem
UNDERGROUND UTILITIES CHECKLIST
Utility
Power
Telephone
Gas
Locator/Contact Person
Miss Utilities
Phone#
Water
Sewer
same
same
Call made by: Donna Wilson. Ticket Number 574-837.
2
Also, if known, list
-50
odor)
EXPOSURE
eem
LIMIT
25 eem
50 eem
100 eem
0.5 mg/m'
0. 01 mg/m'
0. 05 mg/m'
25 eem
100 pem
50 eem
Date of Location
7-28-98
same
same
•
ID# NCO 001 606 250
Facility Description: Size unknown Buildings unknown
Disposal Methods Being Investigated _B_u_r_i_·e_d_d_r_u_rn_s_. ______________ _
Unusual Features on Site (dike integrity, power lines, terrain, etc.)
none known
History of the Site: The site was a former textile mill and the drums were
discovered while conducting a site visit to JFD Electronics.
C. HAZARD EVALUATION
The site can be toured and sampled in level D protection. PE or PVC gloves
will be worn while collecting soil or water samples, PE or PVC gloves over
nitrile gloves will be worn if discolored soil or sludge is encountered.
The OVA will be used to monitor breathing zone air while augering. If OVA
readings exceed 5 meter units in the breathing zone, stand upwind of the
hole for a few minutes, then sample the air again. If the breathing zone
concentration does not drop to below 5 mu after 10 minutes, fill in the
hole and evacuate that area. Tyvek suits (saranex in wet conditions) will
be worn while augering. Chemically resistant knee length boots will be worn
on site. The draft SOPs for the operation of the Little Beaver
will be followed while installing the monitoring wells. PPE will consist
of PVC gloves (nitrile if doscolored soil or sludge is encountered), hard
hats, chemically resistant knee length boots, and a tyvek suit (saranex in
wet conditions) for the person changing the augers. Ear plugs are
recommended. A tyvek suit will be carried to the surface water sampling
locations and worn if the samples cannot be collected without getting muddy.
D. WORK PLAN INSTRUCTION
Map or Sketch Attached? _y_e_s ____ _
Perimeter Identified? no =----
Command Post Identified? no =----
Zones of Contamination Identified? no -----
Personal Protective Equipment/Level of Protection: ___ c X D
3
•
ID# NCO 001 606 250
Modifications Wear goggles, face shield, and PVC gloves while preparing
acid preserved samples, goggles and PVC gloves while collecting acid
preserved samples. Avoid breathing acid vapors.
Surveillance Equipment:
X
HNU
OVA
Explosirneter
Decontamination Procedures
Detector Tubes and Pumps
02 Meter
Radiation Monitor
Level C -----Respirator wash, respirator removal, suit wash (if needed),
suit removal, boot wash, boot removal and glove removal.
X Level D -----Boot wash and rinse and boot removal, suit removal, glove
and goggle removal.
Modifications Dispose of trash properly, on-site if possible.
Work Schedule/Visit Objectives The purpose of this visit is to determine
if the site poses a threat to the public health or environment because of
releases of contaminants to soil, surface water, groundwater, or air.
Sampling may consist of groundwater, surface water, subsurface soil, and
surface soil sampling.
EMERGENCY PRECAUTIONS
Route of Exposure
E es
Skin
Inhalation
Ingestion
4
First Aid
irrigate immediately
soap and water wash
fresh air and artificial respiration
get medical attention immediately
X
0
ID# NCO 001 606 250
Location of Nearest Phone: unknown (nearby residences/businesses?)
Hospital (Address and Phone Number)
Granville Medical Center, College St. Extention, PO Box 947, Oxford, NC
[phone] -can handle chemically contaminated patients
Emergency Transportation Systems (Phone Numbers)
Fire I 919) 690-3000
Ambulance [phone]
Rescue Squad [phone]
Emergency Route to Hospital Take the access road back to SR 1004, turn
right, and stay on SR 1004 to Route 15/158/96 and turn left. Travel north
approximately 1 mile, the hospital will be on the right.
X
PREVAILING WEATHER CONDITIONS AND FORECAST
EQUIPMENT CHECKLIST
Air purifying respirator
Cartridges for respirator
Eye Wash Unit
X First Aid Kit --x-
X
3 gal. Deionized H20
Rain suit
HNU
OVA
Explosimeter
Radiation Monitor
Decontamination
·Materials
X
X
X
X
X
Gloves (PE/PVC/nitrile/cloth)
Boots/Boot COVers
Coveralls (tyvek/saranex)
Eye Protection (goggles/shield)
Hard Hat
or
Duke University Medical Center
Telephone: [phone]
Box 3024
Durham, NC 27710
ASHEVILLE
704-255-4490
Western NC Poison HENDERSONVILLE
Control Center 70 -2
rgaret R. Pardee
Memorial Hospital
Fleming St., 28739
CHARLOTTE
704-379-5827
DURHAM
1-800-672-1697
GREENSBORO
919-379-4105
safeform.323c
Memorial Mission Hosp. Ext. 555,556
509 Biltmore Ave. 28801
Mercy Hospital
2001 Vail Ave, 28207
Duke Univ. Med. Center
Box 3007, 27710
Moses Cone Hospital
1200 N. Elm St. 27420
HICKORY
704-322-6649
JACKSONVILLE
919-577-2555
WILMINGTON
919-343-7046
5
Catawba Mem. Hosp.
Fairgrove Chur. Rd 28601
Onslow Mem. Hospital
Western Blvd. 28540
New Hanover Mem. Hospital
2131 S. 17th St. 28401
:cFC Pesticide
lisposal
,CD 986 180 883
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i oY
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Perchloroethylene
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula C2 Cl4
Natural Physical State at 25oC liquid
Vapor Pressure 14 mm Hg at 20oC
Melting Point -2 oF/oC Boiling Point 250
Flash Point (open or closed cup) N/A oC/oF
Solubility - H2O 0.015%
1
2
2
oF/oC 2
2
2
Other misc with alcohol, ether,
chloroform, benzene 1 ---
Physical Features: (odor, color, etc.) colorless
liquid with an odor like ether or ·chloroform IP=9.32 eV
(2) OVA Relative Response= 70%
II. TOXICOLOGICAL DATA
suspect human
Standards: 25 ppm(3)TLV 100 ppm(4)PEL carcinogen (2)IDLH
Routes of Exposure: Inhalation, Ingestion, Skin and/or
Eye Contact (2)
Acute/Chronic Symptoms: Irritation of eyes, nose, and
throat, nausea, flushed face and neck, vertigo, dizziness,
incoordination, headache, carcinogen (2)
First Aid: Inhalation: artificial respiration;
get medical attention immediately; Eye contact:
immediately; Skin contact: soap and water wash
immediately.
Ingestion:
irrigate
•
Chemical Name: Perchloroethylene
III. HAZARDOUS CHARACTERISTICS
Reference
A. Combustibility Yes
Toxic by-products
B. Flammability LEL none
No X
UEL
•
none
C. Reactivity Hazard Incompatible with
oxidizers, chemically active metals, such as
lithium, and beryllium & barium; caustic soda;
hydroxide, potash (2)
D. Corrosivity Hazard yes/no pH:
Neutralizing agent:
E. Radioactive Hazard Exposure Rate
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCES
1. The Merck Index, 11th Edition, 1989
2
2
strong
barium,
sodium
2. NIOSH Pocket Guide to Chemical Hazards, 1990
3. Threshold Limit Values and Biological Exposure
Indices for 1997 ACGIH.
4. CFR 1910.1000.
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Toluene (Methyl benzene, toluol)
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula C7H8
Natural Physical State at 25'C liquid
Vapor Pressure 20 mm Hg at 20'C
Melting Point -95'F/'f Boiling Point 110.6'F/'C
Flash Point ( open or closed cup) 4 0 'C/' F
1,2,3,4
1,2,3,4
3
1, 3, 4
1,2,3,4
Solubility - H2O slightly soluble 1,3,4
Other miscible with alcohol, 1,3,4
chloroform, ether, acetone,
glacial acetic acid, carbon
disulfide
Physical Features: (odor, color, etc.) colorless
liquid with an aromatic odor, IP 8.82 eV, (3) derived
from coal tar oil or petroleum Relative response on
HNU = 10
II. TOXICOLOGICAL DATA
Standards: 50 ppm (5) TLV
100 ppm (6) PEL 2000 ppm (4) IDLH
Routes of Exposure:
contact, eye contact
inhalation; ingestion, skin
Acute/Chronic Symptoms:
headache, lassitude, and
Narcotic in high concentrations,
nausea. Chronic: anemia and
dermatitis. (2)
First Aid: Inhalation: artificial respiration;
get medical attention immediately; Eye contact:
immediately; Skin contact: soap and water wash
immediately
Ingestion:
irrigate
• •
Chemical Name: Toluene -------------
III. HAZARDOUS CHARACTERISTICS
Reference
E.
IV.
A. Combustibility Yes X
Toxic by-products
No
B. Flammability LEL 1.0% UEL 7.0%
C. Reactivity Hazard strong oxidizers
D. Corrosivity Hazard yes/no pH:
Neutralizing agent:
Radioactive Hazard Exposure Rate
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
REFERENCES
(1) The Merck Index, 11th Edition, 1989
(2) Documentation of the TLV, 4th Edition, 1980
3
(3) NIOSH Pocket Guide for Chemical Hazards, 1990
(4) NEPA, Protection Guide on Hazardous Materials,
8th Edition, 1984
(5) Threshold Limit Values and Biological Exposure
Indices for 1997
(6) 29 CFR 1910.1000
4
4
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Xylene, O, M, & P (Dimethyl benzene)
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula ~8__1:!1o '--------1
Natural Physical State at 25°c liquid 1 ----Vapor Pressure 7~9 mm Hg at 20°C 1
Melting Point 1:f.="TT°F/0 c Boiling Point 137-140°F/°C-~l-
Flash Point (open or closed cup) 90/84/81°C/0 I _l __
Solubility - H2O insoluble 1
Other soluble in alcohol, ether 1 ---• and most other organic solvents.
Physical Features: (odor, color, etc.) colorless liquid with
aromatic/ benzene odor. Common solvent for paints and coatings.
IP= 8.5 eV. HNU relative response with 10.2 eV probe= 11.3, OVA
relative response= 111 -116%
II. TOXICOLOGICAL DATA
Standards: 100 ppm (2) TLV
IDLH
100 ppm (3) PEL 1,000 ppm (4)
Routes of Exposure: Inhalation, Ingestion, Skin and/or Eye
contact
Acute/Chronic Symptoms: headache, fatigue, dizziness, lassitude,
narcotic effects in high concentrations (5,6). Chronic effects not
well defined (1).
First Aid: Inhalation: artificial respiration; Ingestion: get
medical attention immediately; Eye contact: irrigate immediately;
Skin contact: soap and water wash immediately.
Chemical Name: Xylene, 0, M, & P
III. HAZARDOUS CHARACTERISTICS Reference
E.
A. Combustibility Yes X No
Toxic by-products
B. Flammability LEL 1.4% UEL 6. 7%
C. Reactivity Hazard strong oxidizers
D. Corrosivity Hazard
Neutralizing agent:
Radioactive Hazard
Background
Alpha particles
Beta particles
Gamma radiation
yes/no
yes/no
yes/no
yes/no
yes/no pH:
Exposure Rate
IV. REFERENCES
(1) The Merck Index, 11th Edition, 1989.
•
1,2,3,4
2
4
(2) Threshold Limit Values and Biological Exposure
Indices for 1997
(3) 29 CFR 1910.1000
(4) NIOSH Pocket Guide to Chemical Hazards, 1990.
5) NFPA, Fire Protection Guide on Hazardous
Materials, 8th Edition, 1984.
(6) Documentation of the TLV, 4th Edition, 1980
•
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Barium (soluble compounds)
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula Ba
Natural Physical State at 25oC
depending on compound
properties vary
Vapor Pressure mm Hg at 20°c
Melting Point --~°F/°C Boiling Point
Flash Point (open or closed cup)
Solubility - H20 vary
Other vary
°C/°F
Physical Features: (odor, color, etc.)
depending on compound(2)
II. TOXICOLOGICAL DATA
Standards: 0.5 mg/m3(3) TLV 0.5 mg/m3(4) PEL
1,100 mg/m3(2) IDLH
Vary
1
2
2
Routes of Exposure:
eye contact
Inhalation, Ingestion, skin and/or
1
Acute/Chronic Symptoms: Upper respiratory irritation, GI
irritation, muscle spasms, slow pulse, premature
contractions of the heart, extrasystoles, hypokalemia,
irritation of eyes, skin burns. (2)
First Aid: Inhalation: artificial respiration; Ingestion:
get medical attention immediately; Eye contact: irrigate
immediately; Skin contact: soap and water wash
immediately.
f)
Chemical Name: Barium
III. HAZARDOUS CHARACTERISTICS
Reference
A. Combustibility Yes No
Toxic by-products
•
• depends on compound
B. Flammability LEL UEL
C. Reactivity Hazard depends on compound
D. Corrosivity Hazard yes/no pH:
Neutralizing agent:
E. Radioactive Hazard Exposure Rate
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCES
1. The Merck Index, 11th Edition, 1989
2. Pocket Guide to Chemical Hazards, NIOSH, 1990
3. Threshold Limit Values and Biological Indices
for 1997 ACGIH.
4. 29 CFR 1910.1000
2
2
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Chromium (VI), insoluble salts
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula varies with compound 1
Natural Physical State at 25°c solid 1
Vapor Pressure N/A mm Hg at 20°c
Melting Point °F/°C Boiling Point
Flash Point (open or closed cup) N/A °C/° F
Solubility -H2O not soluble in water
Other
Physical Features: (odor, color, etc.) Properties vary
depending upon specific compound. Compounds include: zinc
chromate, lead chromate, calcium chromate, etc.
II. TOXICOLOGICAL DATA
1
Standards: 0.01 mg/m3 (2) TLV 0.5mg/m3 (4) PEL 500 mg/m3 (3) IDLH
Routes of Exposure: Inhalation and ingestion
Acute/Chronic Symptoms: Chronic: fibrosis of the lung and
epidemiological studies have shown increased incidence of lung
cancer among workers in the manufacture of chrome pigments
First Aid: Inhalation: artificial respiration; Ingestion: get
medical attention immediately; Eye contact: irrigate
immediately; Skin contact: soap and water wash immediately
•
Chemical Name: Chromium (VI), insoluble salts
III. HAZARDOUS CHARACTERISTICS Reference
A.
B.
C.
D.
Combustibility Yes
Toxic by-products
Flammability
Reactivity Hazard
Corrosivity Hazard
Neutralizing agent:
No X
LEL N/A UEL
strong oxidizers
yes/no pH:
E. Radioactive Hazard
Background
Exposure Rate
Alpha particles
Beta particles
Gamma radiation
yes/no
yes/no
yes/no
yes/no
IV. REFERENCES
1. The Merck Index, 11th Edition, 1989.
2 . Threshold Limit Values and Biological
for 1997 ACGIH
Exposure Indices
3. Pocket Giude to Chemical Hazards, NIOSH, 1990
4. 29 CFR 1910.1000
3
•
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Lead, inorganic dusts
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula Pb 1 ----Natural Physical State at 25°C solid 1 ----Vapor Pressure N/A mm Hg at 20°C 1
Melting Point 32'f:4"°F/°C Boiling Point 1,740°F/°C _1 __ _
Flash Point (open or closed cup) N/A°C/°F
Solubility -H2O N/A
OtherN/A ---------------
Physical Features: (odor, color, etc.) appearance and odor
vary depending upon specific compound.
II. TOXICOLOGICAL DATA
suspected or confermed human
Standards: .05 mg/m3 (2) TLV
N/A (4) IDLH
carcinogen
0.05 mg/m3 (3) PEL
Routes of Exposure:
contact(3)
inhalation, ingestion, eye contact, skin
Acute/Chronic Symptoms:Acute: lassitude, pallor, constipation,
abdominal pain, gingival gum line, tremors. Target organs: GI
tract, CNS, kidneys, blood. (3)
First Aid: Inhalation: artificial respiration; Ingestion: get
medical attention immediately; Eye contact: irrigate immediately;
Skin contact: soap and water wash immediately
•
Chemical Name: Lead, inorganic dusts
III. HAZARDOUS CHARACTERISTICS
Reference
A. Combustibility Yes
Toxic by-products
B. Flammability
C. Reactivity Hazard
D. Corrosivity Hazard
Neutralizing agent:
No X
LEL N/A
None
yes/no
E. Radioactive Hazard Exposure Rate
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCES
UEL
pH:
(1) The Merck Index, 11th Edition, 1989
(2) Threshold Limit Values and Biological Exposure
Indices for 1997 ACGIH.
(3) 29 CFR 1910.1025
(4) Pocket Guide to Chemical Hazards, NIOSH, 1990.
0 •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Methylene Chloride
I. .PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula CH2 Cl2 =~="-----------
Natural Physical state at 25°C _l_i_q~u_i_d _____ _
Vapor Pressure 350 mm Hg at 20°c
Melting Point -139 °F/°C Boiling Point 104 °F 1°C
Flash Point (open or closed cup) ___ ? ____ °C/°F
Solubility - H20 soluble in 50 parts water
Other misible with alcohols,
DMF
ether,
Physical Features: (odor, color, etc.) Colorless liquid with a
chloroform-like odor (2) IP= 11.35 eV. Relative response on
HNU = 9.4. OVA Relative Response= 100%
II. TOXICOLOGICAL DATA
Standards: 50 ppm(3) TLV 25 ppm(4) PEL
suspect human
carcinogen
____ (~3'-'-) IDLH
Routes of Exposure: Inhalation, ingestion, eye contact, skin contact
1
2
2
2
2
1
1
Acute/Chronic Symptoms: Fatigue, weakness, sleepiness, light headedness, numb
and tingling limbs, nausea, eye and skin irritation, vertigo, choking (2)
First Aid: Inhalation: artificial respiration; Ingestion: get medical
attention immediately; Eye contact: irrigate immediately; Skin contact:
soap and water wash immediately
0
Chemical Name: Methylene Chloride
III. HAZARDOUS CHARACTERISTICS
Reference
A.
B.
Combustibility Yes X No
Toxic by-products
Flammability LEL ·12% -----
•
UEL 19%
C. Reactivity Hazard incompatible with strong oxidizers
2
2
2
and caustics, chemically active metals such as Al or Mg powders,
sodium, potassium.
D. Corrosivity Hazard yes/no
Neutralizing agent:
E. Radioactive Hazard
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCES
pH:
(11 The Merck Index, 11th Edition, 1989
Exposure Rate
(2) Pocket Guide to Chemical Hazards, NIOSH, 1990
(3) Threshold Limit Values and Biological Exposure
Indices for 1997, ACGIH
(4) 29 CFR 1910 1052
0 •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Ethyl Benzene
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula CS Hl0 ----------------
Natural Physical State at 25oC liquid
Vapor Pressure 10 mm Hg at 79oF
Melting Point -139oI/oC Boiling Point 277oI/oC
·Flash Point (open or closed cup) 59-64oC/oF
Solubility - H20 0.01%
· Other miscible with usual organic
solvents
1, 2
1, 2
2
1
1, 2
2
1
Physical Features: (odor, color, etc.) colorless,
flammable liquid with an aromatic odor. IP= 8.76 eV
Relative Response OVA= 100%
II. TOXICOLOGICAL DATA
Standards: 100 ppm (3) TLV
2000 ppm (2) IDLH
100 ppm (4) PEL
Routes of Exposure:
contact
Inhalation, Ingestion, Skin/Eye
Acute/Chronic Symptoms:Irritation of the eyes and mucus
membranes, headache, skin problems, sleepiness, coma (2)
First Aid: Inhalation: artificial respiration; Ingestion:
get medical attention immediately; Eye contact: irrigate
immediately; Skin contact: soap and water wash immediately
Chemical Name: Ethyl Benzene
III. HAZARDOUS CHARACTERISTICS
Reference
A. Combustibility Yes X No
Toxic by-products none known
B. Flammability LEL 1. 0% UEL 6.7%
E.
C. Reactivity Hazard Strong oxidizers
D. Corrosivity Hazard yes/no
Neutralizing agent:
Radioactive Hazard Exposure Rate
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
pH:
IV. REFERENCES
( 1) The Merck Index, 11th Edition, 198 9
•
(2) Pocket Guide to Chemical Hazards, NIOSH 1990
2
2
2
(3) Threshold Limit Values and Biological Exposure
Indices for 1997 ACGIH.
(4) 29 CFR 1910.1000.
•
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Trichloroethylene
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula C2 HC13 -----------------
Natural Physical State at 25'C liquid
Vapor Pressure 58 mm Hg at 20'C
Melting Point --~9~9 ___ 'F~/'C Boiling Point
Flash Point (open or closed cup) 32'C/'F
Solubility -H2O 0.1% at 77'F
Other Ether, alcohol, chloroform
1
1
2
2
3
2
1
Physical Features: (odor, color, etc.) Colorless liquid
(unless dyed) with a sweet odor like chloroform lP = 9.45 eV (2)
OVA Relative Response= 70%
II. TOXICOLOGICAL DATA
Standards: 50 ppm (4) TLV
IDLH
potential
human
100 ppm (5) PEL carcinogen(2)
Routes of Exposure:
contact (2)
Inhalation, ingestion, skin and/or eye
Acute/Chronic Symptoms: Acute: Headache, vertigo, visual
disturbance, tremors,
drowsiness, nausea, vomiting, eye irritation, dermititis,
irregular heartbeat,
skin irritation; chronic: carcinogenic (2)
First Aid: Inhalation: artificial respiration; Ingestion: get
medical attention immediately; Eye contact: irrigate
immediately; Skin contact: soap and water wash immediately
Chemical Name: Trichloreothylene
III. HAZARDOUS CHARACTERISTICS
A.
B.
Combustibility Yes X
Toxic by-products
No
Flammability LEL 12.5%
•
Reference
UEL 90%
C. Reactivity Hazard Incompatible with strong caustics:
when acidic reacts with aluminum, chemically active metals,
barium, lithium, sodium, magnesium, titanium.
D. Corrosivity Hazard yes/no pH:
Neutralizing agent:
E. Radioactive Hazard Exposure Rate
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCES
(1) The Merck Index, 11th Edition, 1989
(2) Pocket Guide to Chemical Hazards, NIOSH, 1990
(3) Chemical and Engineering News, December 12, 1988.
(4) Threshold Limit Values and Biological Exposure
Indices for 1997 ACGIH
(5) 29 CFR 1910 .1000
2
3
2
KEY RISK M~~MENT SERVICES, INC.
.· ATTN: STATE ~'QI' · .. . ·P.O. BOX 49129 .
GREENSBORO, NC 27419 COMDCIII
NETWORK,INC.
WORKERS' COMPENSATION MEDICAL AUTHORIZATION
/ Name of Employee/Patient: Last
/ Date ofiniurv:
/ Name of Employer/Company:
Employer Authorization:
First
J Social Securirv Number:
STATE OF NORTH CAROLINA DEHNR
Doctor To Be Seen:
Emplover:
Employee:
Complete this form, and give it to the injured employee before a doctor is seen.
Show this form to the doctor.
Sec. No. 4.0
Rev. N,:,. 4
Date: 8-20-'.
Page 2 of 2
Phvsician: When a referral is necessary -use CompCare Physicians and call 1-800-366-1511, to let
the state agency claims representative know that the patient is being referred.
SEN'D BILL DIRECTLY TO KEY RISK MANAGEMENT SER VICES, INC.
• • NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WASTE MANAGEMENT
July 27, 1998
Mr. Mitchell Arnold
Environmental Health Supervisor
Granville-Vance District
115 Charles Rollins Road
Henderson, NC 27 5 3 6
RE: Removal Evaluation/Site Inspection
Cristex Drum Site, NCD00I606250
Dear Mr. Arnold:
David Lilley of the NC Superfund Section spoke with you to notify you that the NC
Superfund Section will conduct a site inspection of the subject site located in Granville County,
North Carolina. The inspection will be conducted from August I 0-14, 1998 by Donna Wilson of
the NC Supcrfund Section.
The purpose of the inspection is to detennine if the site poses a hazard to public health or
the environment because of releases of contaminants to soil, surface water, groundwater, or air. The
inspection team will take samples on and around the site to detennine if a hazardous condition
exists. Additionally, they will locate all nearby water supplies (surface and groundwater, community
and private) and any close sensitive environments, schools, and day care centers.
This inspection is not an emergency situation but is a normal step in the evaluation of all
uncontrolled and unregulated potential hazardous waste sites in North Carolina. You may want to
have your representative meet the inspection team at the site. If so, please contact Donna Wilson
at (919) 733-280 I, ext. 3 I 7 and she will coordinate a meeting.
If the inspection indicates the need for future study of the site, we will contact your office
to advise. If you have any questions, please don't hesitate to call David Lilley or me at (919) 733-
2801.
Enclosures
cc: Phil Prete
Doug Holyfield
Pat Williamson
Scott Ross
David Lilley
Donna Keith
Sincerely,
)1/:J?fl\.__-----'
Pat DeRosa, Head
Site Evaluation and Removal Branch
NC Superfund Section
401 OBERLIN ROAD, SUITE 150, RALEIGH, NC 27605
PHONE[phone] FAX[phone]
AN EQUAL OPPORTUNITY/ AFFIRMATIVE ACTION EMPLOYER· SOo/o RECYCLED/I 0% POST-CONSUMER PAPER
Federal.
~rip Notification & AuthorizaA
Prepared by: D0/11/;,Z_,, lUi/9Jf1 Today's Date: ?-ZZ--98
• Use Ol:.id: Ink or Typcwri1cr only-St~ff 10 fill out first :? blocks only.
Site Trip.
Date of Trip: Au.0-10-li7!1'JS' ·-If trip date changed or cancelled note below:
Trip Date Changed To: Cancelled: --
.....
_j,v/VI SH~ NCO#: Oo{ 60(, Z'-:V ·site Name: Cr,::,tc)(·
City: ox&J. County: GY<f/1 v/l I~
. -
S//c, / !<~,ii &Viz.Lr;:/,~ Reason for Trip: lr1:fZc. +(o.r1
Name of Hotel (Overnight Trip): Hotel Telephone Number: ( )_-
Authorized by: fl'JJ?_/~ -Industrial 1-lyc,ricn~
Project Team Leader: DCYl()tL lu//5of)
Dw', d i!k:lf. >(7'-~ rr l/ Zi'11 11. Jbv.,.,e ft-,_ s6_;1{e,
JrvW..rf-f!ar /:.c,--Assistants: I vc.; Ru rri/2"/. ' OU C, (}'I CV re.-' ~ -J ... -

-
. --
Attach To Notification Form: 1 copy each: Preliminary Assessment Form (First page only) Submit to the Site Map
Industrial Hygienist PA Transmittal Letter
(Please list appropriate County Health Department contact pcr..on to call to advise of trip)
Environmental Supervisor or Health Director to call: r~ .. efl•,-i-,bf I/ 1,4:,"riJ
(Note if Dr., M.P., etc.)
Telephone Number: ('l;q)'ffQ : 711,:,_,.
Notes: Health Department Official Contacted: iJ?;/cfce.!/ t&:nal/
Back Up Letter Required: Yes /,... No
No/:,{,e,} /!1r. Jc/1,;/j i/Y\-'7-J.'1-'iff (IJL1L)
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NOR ·t.-{\
.·i· ...
• NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
July 14, 1998
Mr. Philip H. Vorsatz
NC CERCLA Project Officer
US EPA Region IV Waste Division
61 Forsyth St., 11th Floor
Atlanta, GA 30303-3104
DIVISION OF WASTE MANAGEMENT
SUBJECT: Sampling Plan for the Preliminary Assessment/Site Inspection
(PA/SI)
Cristex Drum Site
NCO 001 606 250
Oxford, Granville County, NC
Dear Mr. Vorsatz:
This letter contains the proposed sampling plan for the Preliminary
Assessment/Site Inspection (PA/SI) of Cristex Drum Site in Granville County,
NC. After reviewing the available file information and after a removal (January
1997) and two reconnaissance trips (3-9-98 and 6-1-98), it is apparent that a
combined PA/SI should be conducted and that sampling is needed in order to
more fully characterize the groundwater, surface water, and soil exposure
pathways. I plan to perform the sampling the week of August I 0, 1998.
The subject property was the location of a textile mill from 1965 to 1986,
under various owners and operators. The operation involved knitting, dyeing, and
finishing of tricot and knit fabrics (acetate, nylon, and polyester). A number of
dyes were used in the process and the resulting wastewaters were discharged to an
underground pipe, which drained to a pretreatment lagoon near the facility. The
lagoon is approximately 0.6 acre in size and had a reported depth of 5 feet. The
wastewaters were treated by aeration in the lagoon, for a designed retention time
of 3 days, prior to discharge to the City of Oxford sewer system. Earlier this year,
the owner of the property hired an environmental firm, Leonhardt Environmental,
to close out the lagoon. The consultant analyzed the water and the sludge in the
lagoon prior to digging out the sidewall of the lagoon on the north side, releasing
the water to the intermittent stream. Runoff from the source areas which was
401 OBERLIN ROAD, SUITE 150, RALEIGH, NC 27605
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY/ Af'FIRMATJVE ACTION EMPLOYER -50% RECYCLED/10% POST-CONSUMER PAPER
Mr. Philip H. Vorsatz
July 14, 1998
Page 2
• •
previously entering the City's sewer system is now entering the intermittent stream north of
the facility property. The property owner and the consultant have been instructed
not to remove the lagoon contents or close out the lagoon until further notice.
Southeast of the lagoon in an unfenced area is a former drum burial site. The area was
discovered in 1994 by Geraghty & Miller, an environmental services firm, while investigating
the area surrounding the JFD/Channel Master NPL site, which is located directly north of the
Cristex property. In January 1997, EPA conducted a removal action of the drum burial site.
Contaminated soil and 137 drums were removed, 25 of which were exhumed and 112 were
empty and on the ground surface. The contents of the drums were analyzed and found to
contain chlorinated solvents, petroleum products, phenols, and elevated lead. Although the
burial site appears to be located on the Cristex property, the owner of the Cristex property
does not agree.
Adjacent to the lagoon and approximately 150 feet north of the former drum disposal
area is a dir, berm approximately 4 feet high and 90 feet long. A magnetometer survey
revealed small anomalies. A request has been made to EPA for an exploratory dig of the area
to determine if drums may be buried in the berm.
Two vertical above ground storage tanks behind (north of) the facility contained #6
fuel oil to fuel the boilers for the facility. The tanks have 20,000 and 30,000 gallon capacities
an<l ·apparentiy still contain liquid. In 1993, a spill of approximately 14,000 gallons of the fuel
oil was reported to the North Carolina Department of Environment, Health, and Natural
Resources.' The fuel oil entered the nearby drainage ditch, which diverted the oil to the
abandoned lagoon. Clean-up activities were conducted to collect as much of the oil as
possible.
During the operation of the facility, it is reported that drums and vats of dyes,
chemicals, and oils used in the process were stored on a concrete pad on the cast side of the
facility. Runoff from this area is diverted to a drainage ditch that empties into the
pretreatment lagoon. Discharge from the rnoftop air pollution control devices (mesh pad mist
eliminators on tenter frames), consisting of water and finishing oils, also entered the drainage
ditch.
A barren area with little or no vegetation has existed cast of the lagoon since at least
1977. The area is approximately 0.5 acre in size and has one to three feet high sidewalls on
the north, west, and south sides, as if the area were at one time an old lagoon or a soil borrow
area. The east side of the barren area is lower in elevation and is level with the surrounding
terrain. This area is marshy and seeps may be emanating from the ground.
Mr. Philip H. Vorsatz
July 14, 1998
Page 3
•
· Since closure of the textile operation in 1986, the owner has rented the building for use
as a warehouse and distribution center. A drug store company, CVC, is the current occupant.
Groundwater monitoring wells have been installed and sampled on the Cristex
property, as part of the investigation of the JFD/Channel Master NPL site. Analysis indicates
that groundwater within the vicinity of the former drum disposal area and the barren area
contains chlorinated solvents. Some of these chemicals correspond to the chemicals detected
in the groundwater at the JFD site; however, it has not been determined whether the
contaminants on the Cristex property originated from the Cristex site, the JFD site, or both
sites.
Sampling locations on the facility property will include the drum storage pad, the
drainage ditch, the soil surrounding the above ground storage tanks, subsurface soil and
groundwater adjacent to the underground lagoon pipe inlet, the lagoon, the former drur..1
disposal area, and the barren area. Groundwater samples will be collected upgradient and
downgradient of the drum disposal area, the barren area, and the lagoon from tempora,f wells
and existing monitoring wells.
Overland surface water run-off from the source areas flows to the northeast, into an
intermittent stream, and to the lagoon, which now empties to the same intermittent stream.
Surface water sampling will include three samples within the intermittent stream:
downgradient of the lagoon, adjacent to an apartment complex, and upgradient of the P?E;
and two samples within the perennial stream, which contains wetlands.
Groundwater flow from the Cristex site and the JFD/Channel Master site appears to
follow topography and converge along the intermittent stream and flow to the east. Rc:;idents
living downgradient of the two sites, along Lewis Street, are all supplied with water from the
City of Oxford. The City obtains its water from the Ci'.y of Henderson, located approximately
17 miles northeast of Oxford. Most of the residents located south of Industry Drive, along
Lewis Street, are outside of the city limits and utilize well water. One residential well sample
will be sampled during the P NS!. The approximate distance from the Cristex property to the
homes south of Industry Drive is 1500 - l 700 feet.
The attached table more clearly identifies the samples and the rationale for taking these
samples. Maps of the proposed sampling locations are attached.
Mr. Philip H. Vorsatz
July 14, 1998
Page 4
0 •
If you have any questions concerning this sampling plan, please call me at (919) 733-
2801 ext. 317.
Sincerely,
~1t~le; ~~v---
Donna J. Wilson
Environmental Engineer
NC Superfund Section
Approved by: _____________ Date: ___________ _
Paul Vorsatz, Chief, NC Site
Management Section
•
Table of Proposed Samples for Cristex Drum Site PA/SI
NCO 001 606 250
Oxford, Granville County, NC
CD-01-SL Background surface soil V, S, I, Background
PCB
CD-02-SL Background subsurface soil, V, S, I, Background
depth IO -12 feet PCB
. CD-02-GW Temp. well, in front of V, S, I, Background
Cristex building PCB
CD-102-GW Duplicate CD-02-GW V, S, I, Background
PCB
CD-03-SL Onsite drainage ditch from V, S, I, Source characterization
drum storage pad PCB
CD-103-SL Duplicate CD-03-SL V, S, I, Source characterization
PCB
CD-04-SL Onsite surface soil around V, S, I, Source characterization
tanks PCB
CD-05-SL Onsite surface soil around V, S, I, Source characterization
drum storage area PCB
CD-06-SL Subsurface soil, depth IO ft., V, S, I, Source characterization
by underground lagoon inlet PCB
pipe
CD-06-GW Temp. well by underground V, S, I, Establish observed release to
lagoon inlet pipe PCB groundwater
CD-07-SL Barren area surface soil V, S, I, Source characterization
composite PCB
CD-08-SL Barren area surface soil V, S, I, Source characterization
composite PCB
CD-09-SL Downgradient of barren area, V, S, I, Overland flow pathway
surface soil PCB
•
Table of Proposed Samples for Cristex Drum Site PA/SI
Page 2
CD-11-SW Surface water seep from V, S, I, Source characterization
barren area PCB
CD-12-SL Drum area subsurface, depth V, S, I, Source characterization
10-12ft. PCB
CD-112-SL Duplicate CD-12-SL V, S, I, Source characterizati,cn
PCB
CD-13-GW Temp. well, upgradient of V, S, I, Attribution
drum area PCB
CD-14-SD Lagoon sludge inlet, sediment V, S, I, Source characterization
PCB
CD-15-SD Lagoon sludge midpoint, V, S, I, Source cha:·acterizafrm
sediment PCB
CD-16-SD Lagoon sludge outlet, V, S, I, Source characterization
sediment PCB
CD-17-SL Downgradient of lagoon, V, S, I, Overland flow pathway
surface soil PCB
CD-18-SL Downgradient of JFD runoff, V, S, I, Attribution
surface soil PCB
CD-19-GW Temp. well, upgradient of V, S, I, Attribution
lagoon PCB
CD-20-GW Temp. well, downgradient of V, S, I, Establish observed release to
lagoon PCB groundwater
CD-21-SL Intermittent drainage ditch, V, S, I, Attribution, runoff from
upgradient of Oak Ridge PCB upgradient offsite sources
Apts., below RR tracks
CD-22-SL Intermittent drainage ditch, V, S, I, Overland flow pathway, soil
adjacent to Oak Ridge Apts. PCB exposure pathway
CD-23-SL Intermittent drainage ditch, V, S, I, Overland flow pathway, soil
adjacent to Oak Ridge Apts. PCB exposure pathway
•
Table of Proposed Samples for Cristex Drum Site PA/SI
Page3
CD-24-SL Intermittent drn inage ditch V, S, I, Overland flow pathway
surface soil, upgradient of PCB
PPE
CD-24-SW Intermittent drainage ditch V, S, I, Overland flow pathway
surface water, upgradient of PCB
PPE
CD-25-SW Perennial stream surface V, S, I, Attribution
water, upgradient of PPE PCB
CD-25-SD Perennial stream sediment, V, S, I, Attribution
upgradient of PPE PCB
CD-26-SW Perennial stream, surface V, S, I, Establish observed release to
water, below PPE PCB surface water
CD-26-SD Perennial stream, sediment, V, S, I, Establish observed release to
below PPE PCB surface water
CD-27-SW Perennial stream, 0.1 mile V, S, I, Establish observed release to
downstream ofCD-26, PCB wetland
surface water
CD-127-SW Duplicate CD-27-SW V, S, I, Establish observed release to
PCB wetland
CD-27-SD Perennial stream, 0.1 mile V, S, I, Establish observed release to
downstream ofCD-26, PCB wetland
sediment
CD-127-SD Duplicate CD-27-SD V, S, I, Establish observed release to
PCB wetland
CD-28-GW Groundwater sample, V, S, I, Establish observed release to
CMMW20 PCB groundwater
CD-29-GW Groundwater sample, V, S, I, Establish observed release to
CMMW21 PCB groundwater
CD-30-GW Groundwater sample, V, S, I,. Establish observed release to
CMMW16 PCB groundwater
CD-31-GW Groundwater sample, V, S, I, Establish observed release to
CMMWI I PCB groundwater
•
Table of Proposed Samples for Cristex Drum Site PA/SI
Page 4
CD-32-PW Residential well sample
CD-100-TB
CD-100-TB .
Key:
V-volatile organics (Method 8270C)
S -semi-volatile organics
I -inorganics, including metals
PCB -polychlorinated biphenyls
V, S, I,
PCB
V
I
Establish observed ~elease to
drinking water
VOC trip blank
Inorganic preservative blank
1
~
CD-16-SD
\
CD-15-SD
CD-Ol-SL
/
CD-02-SL
CD-02-GW
CD-102-GW
Cristcx Drum· Sire
NCO 001 606 250
Drainage ditch
~
CD-05-SL
I
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. ':•:•:,,.. NCO 001 606 25
~,J{, 'l_...-.., '\', ', _; ·~, .
. . tion Apartment co . 0 . . Wetland CD-27-SW i L , -~,~ .·;
. · . ... , 1 co-27-SD n ;~: ::::-, '· ':::~1/ . .. ~ r--j I ~g:;~;::~~l~~-~iOis~ ,
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Scale: I" -

I

000'
NORTH SUPERFUND
Mr, Philip H. Vorsatz
July 14, I 998
Page 4
ID: • JUL 23'98 15:29 No.005 P.05 •
lfyou huve any questions concerning thi~ ~ampling plan, please cull me at (919) 733-
2801 ext. 317.
Approved hy:
Sincerely,
,-/(()tlt~ (V~{S.v-
Donna J. Wilson
F,nvironmcntal Engineer
NC Superfund Section
n1cJ!tA~l~x_.hn--Date: _2/_;;.. '3-+-/1-'-----'if __
~au! ~&;J/r I
Management Section
NORTH SUPERFUND JUL 23'98 15:25 No.006 P.01 •
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
TO: Dooole WIison
REGION 4
Atlanta Federal Center
61 Forsyth Street, S.W.
Atlanta, Georgie 30303
FACSIMILE TRANSMITTAL COVER SHEET
COMPANY/ORGANIZATION: .uN .... C..i..Di.cf.lllNLC1Bc-----------------
DA TE: Zt23(9B
PHONE NUMBER: FAX NUMBER: 919/733/4811
NUMBER OF PAGES SENT (Including this cover sheet): 11
Please contact the person sending this fax If It Is received poorly or Incomplete.
FROM:
McKenzie Mallary
North Site Management Branch
Waste Management Division
Phone Number: (404} 562-8802
Fax Number: [phone]
COMMENTS: Here Is approved work plan for Crlstex.
To:
From:
Subject:
Date:
MEMORANDUM
File
Donna Wilson T
Environmental Engineer
North Carolina Superfund Section
Magnetometer survey
Cristex Drum Site
Oxford, Granville County
June 11, 1998
•
On June 1, 1998, Dave Mattison and I conducted a magnetometer survey at the
above referenced site. We arrived at the facility at approximately 9:30 and met with Derr
Leonhardt of Leonhardt Environmental, consultant for George Christiansen. Mr.
Leonhardt stated that the sidewall in the lagoon next to the sewer inlet had been cut out to
allow the lagoon to drain. Samples were taken of the surface water and the sludge before
the surface water was discharged. He said that the Water Quality Division reviewed the
analysis and did not object to the discharge of the water to the tributary to Fishing Creek.
He gave me a copy of the analysis.
We walked to the former drum site, the barren area, and the lagoon. The lagoon
still contains water throughout the bottom, apparently caused by a low permeable layer
and/or slope of the bottom of the lagoon away from the sidewall opening. The area is
overgrown with briars, brush, and blackberries, which made it very difficult to locate the
berm.
Beginning at the south end of the berm, we began marking locations with wooden
stakes for magnetometer readings. We first placed stakes on the crest of the berm, every
five feet, in a straight line, N 20° W, from the south end of the berm to the north end, with
the use of a 100 foot tape measure (row c). We placed 20 stakes, which extended 95 feet.
Although I had initially estimated the berm length to be approximately 30 feet during the
March 1998 reconnaissance, on this day it was not possible to determine the distinct
boundaries of the berm due to the thick vegetation, approximately 3 to 5 feet high. The
north, south, and east edges of the berm were gradually sloped, but the western edge was
more sloped. Each station was numbered from 1 to 20, south to north. We then returned
to the south end of the berm and placed stakes perpendicular to the original line, at each
station, on 5 foot centers, from station 2 to station 8, with the use of a compass (rows b
Memorandum
Cristex Drum Site
Page 2
•
and d). Adjacent points for station 1 were not marked because it did not appear to be part
of the berm. We stopped at station 8 because there were not enough wooden stakes to
continue.
Magnetometer readings were obtained for the 22 marked points. Dave Mattison
operated the magnetometer and I recorded the readings. The magnetometer is
manufactured by Geometrics and its model number is G816/826A, Serial No. 6527. The
magnetometer is worn in straps over the shoulders and the magnet is placed vertical on
top of a 4 foot rod. Three readings were taken at each point, so that an average could be
obtained. After taking the first 3 readings, it was discovered that the box we had carried
to the berm containing some metal objects (hammer, compass, etc.) was close to station I.
The box was moved approximately 20 feet away. After completing the readings for
stations 1 -8, we returned to stations 1 and 2 and took new readings, to correct for any
influence of the objects in the box.
At approximately 11 :30, while we were obtaining the readings described above,
Derr Leonhardt left the site.
Dave Mattison and I removed some of the stakes from stations I - 8 to reuse for
additional stations. We then measured and placed wooden stakes for stations 9 -14,
again using the compass to place the stakes perpendicular to the center line c. We were
not able to place stakes on row d at stations 13 and 14 because the briars and brush were
too thick. A new western row, a, was added for those stations, which were on the side
slope of the berm.
We broke for lunch at 12:15 and returned to the site at 1 :15.
Readings were taken for stations 9 and 10 and we observed that the numbers were
lower on the eastern side of the berm (row b) in comparison to the readings for the other
rows. Readings on row b were measured with the magnet to the left (west) of the
instrument for convenience in dealing with the briars on stations 5 -9, while the readings
on rows c and d were measured with the magnet to the right (east) of the instrument. We
tested one point on station 10 by taking measurements with the magnet in both positions
and discovered a gamma difference of 40. All subsequent measurements were consistent
with positioning and row b readings from stations 5 -9, which were influenced by the
thick briars, were remeasured. Measurements taken on stations I - 4 were not affected.
After completing the readings for row b on stations 5 - 9 and the readings for
stations 9 -14, some of the stakes were removed and reused on stations 15 -20. On
stations 15, 18, 19, and 20, row d was deleted and row a was added because of the
Memorandum
Cristex Drum Site
Page 3
shape of the berm.
•
After completing all magnetometer readings, Dave Mattison scanned the metal
detector in a sweeping motion over the study area. One precise "hit" was found between
stations 19 and 20 on the slope of the berm. We could find no visible source at the
ground surface. The spot was marked with a wooden stake. No other anomalies were
noted on the berm. We also scanned the barren area with the metal detector and found no
anomalies.
After driving by the Oak Ridge apartment complex and Maple Street, the
residential street closest to the surface water point of probable entry, we left Oxford at
approximately 3 :45.
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;l. ---7-------f------+-----J..----l-----·~: ;_.
t'~ ~. ------t----t-----+----f-------'+----
•
SITE HEALTH AND SAFETY PLAN
A. General Information
Site Name ~:..l.lil..l~-----------------ID# NCO 001 606 250
Location Cornor of Industrial Dr, and Pine Tree
Rd, Oxford, Granville County, NC
Proposed Date of Investigation ~J~uuoue._1...._._..1~9~9~8,_ ______ _
Date of Briefing uM~a~y'-'2~9'-'-._.14949~8'----------------
Date of Debriefing ~J~uuoue.....,2..__._._..1~9~9~8'---------------
Nature of Visit (check one): On-Site Reconnaissance
Off-Site Reconnaissance
Sampling
Sampling Overview
Remediation Overview
•
Health Department Official contacted Ms, Anita Paul for Mitchell Arnold
Date of Contact
Site Investigation Team: All site personnel have read the Site Health and
Safety Plan and are familiar with its provisions.
Personnel Responsibilities Signature
Team 1 Donna Wilson team leader, recon
Team 1 David Mattison reconnaissance
Plan Preparation:
Prepared By: David Lilley. Industrial Hygiene consultant
Reviewed By: Jack Butler, Superfund Section Chief
•
B. SITE/WASTE CHARACTERISTICS
Waste Type(s) ___..lL_Liquid ___..lL_Solid ___ Sludge ___ Gas ____x__vapor
Characteristics ___ Corrosive ___..lL_Ignitable ___ Radioactive
__x__volatile ___..lL_Toxic ___ Reactive ___ Other
List Known or Suspected Hazards (physical, chemical biological or
radioactive) on Site and their toxicological effects.
chemical amounts
HAZARD WARNING PROPERTIES
Also, if known, list
EXPOSURE
LIMIT
Tetrachloroethene Odor Threshold /OT) -4.68 -50 ppm 25 ppm
Toluene
Xylene
Barium
Chromium
Methylene Chloride
Ethvlbenzene
Trichloroethvlene
OT 0,17 -40 ppm
OT o.os -200 ppm
OT= no data
OT -no data
OT -no data
OT-25-30 oom tcan adaot to odor)
OT
OT
0.2s -200 ppm
0.2 -400 ppm
UNDERGROUND UTILITIES CHECKLIST
Utility Locator/Contact Person Phone#
Power
Telephone
Gas
Water
Sewer
Call made by:
N
2
so 1212m
lQQ QQID
0.5 mgLm3
0.1 mg[m3
0.05 mg{m3
25 oom
100 ppm
so ppm
Date of Location
•
ID# NCO 001 606 250
Facility Description: Size unknown Buildings unknown
Disposal Methods Being Investigated ~B~u~r~i~e~d"-'dw..r~uilm~sw•~-------------
Unusual Features on Site (dike integrity, power lines, terrain, etc.):
HiStory of the site: The site was a former textile mill and the drums were
discovered while conducting a site visit to JFD Electronics.
C. HAZARD EVALUATION
The site can be toured in level P nrotection. No samolina will be
conducted at this time, Steel toed work boots will be worn while touring
D. WORK PLAN INSTRUCTION
Map or.sketch Attached? .v~e=s~---
Perimeter Identified? ~o~o~----
Command Post Identified?
Zones of Contamination Identified?
Personal Protective Equipment/Level of Protection: ___ C
Modifications
3
Surveillance Equipment:
HNU
OVA
Explosimeter
Decontamination Procedures
•
ID# NCO 001 606 250
Detector Tubes and Pumps
02 Meter
Radiation Monitor
_____ Level C Respirator wash, respirator removal, suit wash (if needed),
suit removal, boot wash, boot removal and glove removal.
-~--_Level D Boot wash and rinse and boot removal, suit removal, glove
and goggle removal.
Modifications Dispose of trash orooerlv, on-site if possible,
work schedule/Visit Objectives The purpose of this visit is to determine
if the site poses a threat to the public health or environment because of
releases of contaminants to soil, surface water, groundwater, or air,
No sampling will be conducted at this time, sampling may take place on a
te dat
EMERGENCY PRECAUTIONS
Route of Exposure
Inhalation
rnaestion
4
First Aid
irrigate immediately
soap and water wash
fresh air and artificial respiration
get medical attention immediately
x
•
ID# NCO 001 606 250
Location of Nearest Phone: unknown (nearby residences/businesses?}
Hospital (Address and Phone Number)
Granville Medical center, College St, Extention, PO Box 947, Oxford, NC
r 919) 693 5115 can handle chemically contaminated patients
Emergency Transportation Systems (Phone Numbers)
Fire 19191 690-3000
Ambulance 19191 690-3000
Rescue Squad 1919) 690-3000
Emergency Route to Hospital Take the access road back to SR 1004, turn
right, and stay on SR 1004 to Route 15/158/96 and turn left, Travel north
approximately 1 mile, the hospital will be on the riaht,
PREVAILING WEATHER CONDITIONS AND FORECAST
EQUIPMENT CHECKLIST
Air purifying respirator
Cartridges for respirator
Eye Wash Unit
First Aid Kit
3 gal. Deionized H20
Rain suit
HNU
OVA
Explosimeter
Radiation Monitor
Decontamination
Materials
Gloves (PE/PVC/nitrile/cloth)
Boots'/Boot Covers
Coveralls (tyvek/saranex)
Eye Protection (goggles/shield)
Hard Hat
-------...,-------·--·----------
Poison Control Center -State Coordin~~r
Duke University Medical Center /
Telephone: [phone] /
Sox 3024 //
Du~~
ASHEVILLE
704-255-4490
Western NC Poison HENDERSONVILLE
Control Center 704-693-6522
Margaret R. Pardee
Memorial Hospital
Fleming St., 28739 Memorial Mission Hosp. Ext. 555,556
509 Biltmore Ave. 28801
CHARLOTTE
704-379-5827
Mercy Hospital
2001 Vail Ave, 28207
DURHAM Duke Univ. Med. Center
1-800-672-1697 Box 3007, 27710
GREENSBORO Moses Cone Hospital
919-379-4105 1200 N. Elm St. 27420
safeform.323b
HICKORY
704-322-6649
JACKSONVILLE
919-577-2555
WILMINGTON
919-343-7046
5
Catawba Mem. Hosp.
Fairgrove Chur. Rd 28601
Onslow Mem. Hospital
Western Blvd. 28540
New Hanover Mem. Hospital
2131 S. 17th St. 28401
/
CCFC Pesticide
Di.spos:al
NCO 986 180 883
JFD Electronics
(Channel Master) -\!~::::=~:-=~~~~::.C':fa-,/-~~=fj\J!lsi
-.icr~'12 263 02s
"19\=a;,-'--ifn~~~~f,,--ti,;a/Z-+-\,~~
17'30"
\
• •
TO BE COMPLETED BY PROJECT MANAGER
PROJECT MANAGER: Donna Wilson PROJECT: ~c&rji~s~t~e~x~-------
INVESTIGATION DATE: June 1. 1998
RECONNAISSANCE ___lL_ SAMPLING VISIT ___ REMEDIATION/SAMPLING OVERVIEW
Respirator Worn By Approximate Time in Respirator
Air Monitoring Data (Include Calibration Reading)
HNU:
OVA:
Explosimeter:
Radiation Meter:
Were there any injuries? If yes, explain: ______________ _
If the maximum personal protective equipment as outlined in the Hazard
Evaluation Section was not used, please justify:
Visitors Present Organization Represented
Signature
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Perchloroethylene
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula __,.c-~C,....:,.__ __________ _
Natural Physical State at 25oC liquid
Vapor Pressure -~1~4 __ mm Hg at 20oC
2
Melting Point --~2 __ oE/oC Boiling Point 250 oE/oC ~2 __
Flash Point (open or closed cup) N/A oC/oF
Solubility -H,o 0.015% 2
Other misc with alcohol. ether.
chloroform. benzene
Physical Features: (odor. color. etc.) colorless
liquid with an odor like ether or chloroform IP=9.32 ev
/2} OVA Relative Response= 70%
II. TOXICOLOGICAL DATA
suspect human
standards: 25 ppm/3\TLV 100 ppm/4)PEL carcinogen /2\IDLH
Routes of Exposure: Inhalation. Ingestion. skin and/or
Eye contact /2}
Acute/Chronic Symptoms: Irritation of eyes. nose. and
throat. nausea. flushed face and neck. vertigo. dizziness.
incoordination. headache. carcinogen <21
First Aid: Inhalation: artificial respiration;
get medical attention immediately; Eye contact:
immediately; Skin contact: soap and water wash
immediately.
Ingestion:
irrigate
•
Chemical Name: Perchloroethylene
III. HAZARDOUS CHARACTERISTICS
Reference
A. Combustibility Yes
Toxic by-products
B. Flammability LEL none
No _x_
UEL
•
none
c. Reactivity Hazard Incompatible with
oxidizers. chemically active metals. such as
lithium. and beryllium & barium; caustic soda;
hydroxide. potash 12}
D. Corrosivity Hazard yes/no pH:
Neutralizing agent:
E. Radioactive Hazard
Background
Alpha particles
Beta particles
Gamma radiation
IV. REFERENCES
yes/no
yes/no
yes/no
yes/no
Exposure Rate
1. The Merck Index. 11th Edition. 1989
__ 2_
2
strong
barium.
sodium
2, NIOSH Pocket Guide to Chemical Hazards. 1990
3, Threshold Limit Values and Biological Exposure
Indices for 1997 ACGIH,
4. CFR 1910.1000.
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Toluene (Methyl benzene. toluoll
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula C7H8
Natural Physical State at 25°C liquid
Vapor Pressure ____2_Q_ mm Hg at 20°c
Melting Point -95°F/0 c Boiling Point
Flash Point (open or closed cup) 40
Solubility -H20 slightly soluble
110. 6°Ff°C
°C/°E
1.2.3.4
1.2.3.4
1.3.4
1.2.3.4
1.3.4
Other miscible with alcohol. 1.3.4
chloroform. ether. acetone.
glacial acetic acid. carbon
disulfide
Physical Features: (odor. color. etc,) colorless
liquid with an aromatic odor. IP 8.82 ev. /3) derived
from coal tar oil or petroleum Relative response on
II. TOXICOLOGICAL DATA
Standards: 50 ppm (5) TLV
100 ppm (6) PEL 2000 ppm (4) IDLH
Routes of Exposure:
contact. eye contact
inhalation; ingestion. skin
Acute/Chronic Symptoms:
headache. lassitude. and
Narcotic in high concentrations.
nausea. Chronic: anemia and
dermatitis, C 21
First Aid: Inhalation: artificial respiration;
get medical attention immediately; Eye contact:
immediately; Skin contact: soap and water wash
immediately
Ingestion:
irrigate
•
Chemical Name: =T=o~l=u~e~n~e~--------
III. HAZARDOUS CHARACTERISTICS
Reference
•
A. Combustibility Yes x_ No
Toxic by-products
....L_
B. Flammability LEL ~ UEL 7.0%
c. Reactivity Hazard strong oxidizers
D. Corrosivity Hazard yes/IJQ_ pH: --
Neutralizing agent:
E. Radioactive Hazard Exposure Rate
Background yes/ng_
Alpha particles yes/ng_
Beta particles yes/ng_
Gamma radiation yes/DQ
IV. REFERENCES
Ill The Merck Index. 11th Edition. 1989
12\ Documentation of the TLV. 4th Edition. 1980
/3\ NIOSH Pocket Guide for Chemical Hazards. 1990
14\ NEPA. Protection Guide on Hazardous Materials.
8th Edition. 1984
15\ Threshold Limit Values and Biological Exposure
Indices for 1997
16\ 29 CFR 1910.1000
4
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Xylene. o. M. & P (Dimethyl benzene)
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula ~8_tl10--------
Natural Physical State at 25°C liquid
Vapor Pressure 1::5L mm Hg at 20°c
Melting Point 13-14°F/0
~ Boiling Point 137-140°F/0
~ __l_
Flash Point (open or closed cupl 90/84/81°C/0 E
Solubility -H,o insoluble 1
Other soluble in alcohol, ether
and most other organic solvents.
Physical Features: (odor, color, etc.) colorless liquid with
aromatic/ benzene odor. common solvent for paints and coatings.
IP= 8.5 ev. HNU relative response with 10.2 ev probe= 11.3. OVA
relative response= 111 -116%
II. TOXICOLOGICAL DATA
Standards: 100 ppm (2) TLV
IDLH
100 ppm (3) PEL 1.000 ppm (4)
Routes of Exposure: Inhalation. Ingestion. Skin and/or Eye
contact
Acute/Chronic Symptoms: headache. fatigue. dizziness. lassitude.
narcotic effects in high concentrations (5.6). Chronic effects not
well defined r11.
First Aid: Inhalation: artificial respiration; Ingestion: get
medical attention immediately; Eye contact: irrigate immediately;
Skin contact: soap and water wash immediately.
•
Chemical Name: Xylene. o. M. & P
III. HAZARDOUS CHARACTERISTICS Reference
E.
A. Combustibility Yes _x No
Toxic by-products
B. Flammability LEL 1.4% UEL .2..-....ll_
c. Reactivity Hazard strong oxidizers
D. Corrosivity Hazard
Neutralizing agent:
Radioactive Hazard
Background yes/oo
Alpha particles yes/oo
Beta particles yes/oo
Gamma radiation yes/oo
yes/no pH:
Exposure Rate
IV. REFERENCES
111 The Merck Index. 11th Edition. 1989.
•
1.2.3.4
2
/21 Threshold Limit Values and Biological Exposure
Indices for 1997
/31 29 CFR 1910.1000
/41 NIOSH Pocket Guide to Chemical Hazards. 1990.
51 NFPA. Fire Protection Guide on Hazardous
Materials. 8th Edition. 1984.
/61 Documentation of the TLV. 4th Edition. 1980
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Barium (soluble compounds)
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula
Natural Physical State at 25oC
depending on compound
properties vary
Vapor Pressure mm Hg at 20°c
Melting Point ___ °F/°C Boiling Point ___ °Ff°C
Flash Point (open or closed cup) _°C/°F
Solubility - H2O vary
Other
Physical Features: (odor, color, etc.)
depending on compound(2)
II. TOXICOLOGICAL DATA
Standards: 0.5 mg/m3(3) TLV 0.5 mg/m3(4) PEL
1.100 mg/m3(2) IDLH
vary
__l__
Routes of Exposure:
eye contact
Inhalation. Ingestion. skin and/or
Acute/Chronic Symptoms: Upper respiratory irritation. GI
irritation. muscle spasms. slow pulse. premature
contractions of the heart. extrasystoles. hypokalemia.
irritation of eyes. skin burns. C2l
First Aid: Inhalation: artificial respiration; Ingestion:
get medical attention immediately; Eye contact: irrigate
immediately; Skin contact: soap and water wash
immediately.
•
Chemical Name: Barium
III. HAZARDOUS CHARACTERISTICS
Reference
A. Combustibility Yes No
Toxic by-products
•
depends on compound
B. Flammability LEL UEL
C. Reactivity Hazard depends on compound
D. Corrosivity Hazard yes/no pH:
Neutralizing agent:
E. Radioactive Hazard Exposure Rate
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCES
1. The Merck Index. 11th Edition. 1989
2. Pocket Guide to Chemical Hazards. NIOSH. 1990
3. Threshold Limit values and Biological Indices
for 1997 ACGIH.
4. 29 CFR 1910.1000
__ 2_
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Chromium /VI}. insoluble salts
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula varies with compound
Natural Physical State at 25°C solid
Vapor Pressure NIA mm Hg at 20°c
Melting Point ---~=°F/°C Boiling Point
Flash Point (open or closed cup)
Solubility -H20 not soluble in water
Other
Physical Features: (odor. color, etc.) Properties vary
depending upon specific compound. Compounds include: zinc
chromate. lead chromate. calcium chromate. etc.
II. TOXICOLOGICAL DATA
Standards: 0.01 mg/m3 (2) TLV 0.5mg/m3 (4) PEL 500 mg/m3 (3) IDLH
Routes of Exposure: Inhalation and ingestion
Acute/Chronic Symptoms: Chronic: fibrosis of the lung and
epidemiological studies have shown increased incidence of lung
cancer among workers in the manufacture of chrome pigments
First Aid: Inhalation: artificial respiration; Ingestion: get
medical attention immediately; Eye contact: irrigate
immediately; Skin contact: soap and water wash immediately
• •
Chemical Name: Chromium /VI}. insoluble salts
III. HAZARDOUS CHARACTERISTICS Reference
A. Combustibility Yes _ No~
Toxic by-products
B. Flammability LEL NIA UEL
c. Reactivity Hazard strong oxidizers
D. Corrosivity Hazard
Neutralizing agent:
E. Radioactive Hazard
Background
Alpha particles
Beta particles
Gamma radiation
IV. REFERENCES
yes/no
yes/no
yes/no
yes/no
yes/no
pH:
Exposure Rate
1. Index. 11th Edition. 1989.
__ 3
2 •
The Merck
Threshold Limit Values and Biological Exposure Indices
for 1997 ACGIH
3. Pocket Giude to Chemical Hazards. NIOSH. 1990
4. 29 CFR 1910,1000
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Lead, inorganic dusts
I. PHYSICAL/CHEMICAL PROPERTIES
Chemical Formula
Natural Physical State at 25°C solid
Vapor Pressure ...Jill,. mm Hg at 20°c
Reference
Melting Point 327.4°F/°C Boiling Point 1.740°F/°C
Flash Point (open or closed cup) N/A°C/°F
Solubility - H2O ---1:li.A
Other
Physical Features: (odor, color, etc.) appearance and odor
vary depending upon specific compound.
II. TOXICOLOGICAL DATA
suspected or confermed human
Standards: .05 mg/m3 (2) TLV
N/A (4) IDLH
carcinogen
0.05 mg/m3 (3) PEL
Routes of Exposure:
contact(3)
inhalation. ingestion. eye contact. skin
Acute/Chronic Symptoms:Acute: lassitude. pallor. constipation.
abdominal pain. gingival gum line. tremors. Target organs: GI
tract. CNS. kidneys. blood.(3)
First Aid: Inhalation: artificial respiration; Ingestion: get
medical attention immediately; Eye contact: irrigate immediately;
Skin contact: soap and water wash immediately
•
Chemical Name: Lead. inorganic dusts
III. HAZARDOUS CHARACTERISTICS
A. combustibility Yes
Toxic by-products
B. Flammability
C. Reactivity Hazard
D. Corrosivity Hazard
Neutralizing agent:
No __x_
LEL N/A
None
yes/no
•
Reference
UEL
pH: --
E. Radioactive Hazard Exposure Rate
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCES
(1) The Merck Index. 11th Edition. 1989
(2) Threshold Limit Values and Biological Exposure
Indices for 1997 ACGIH.
(3) 29 CFR 1910.1025
(4) Pocket Guide to Chemical Hazards, NIOSH. 1990.
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Methylene Chloride
I. PHYSICAL/CHEMICAL PROPERTIES
Chemical Formula CH2____Ql2•-----------
Natural Physical State at 25°C ~l~i~q~u~i~d~----
Vapor Pressure 350 mm Hg at 20°C
Melting Point -139 °F/°C Boiling Point
Flash Point (open or closed cup)
solubility -H20 soluble in so parts water
other misible with alcohols, ether.
F
Reference
Physical Features: (odor, color, etc.) Colorless liauid with a
chloroform like odor (2) IP -11.35 ev, Relative response on
HNU = 9,4, OVA Relative Response= 100%
II. TOXICOLOGICAL DATA
Standards: 50 ppm/3) TLV 25 ppm/4) PEL
suspect human
carcinogen
Routes of Exposure: Inhalation, ingestion, eve contact, skin contact
Acute/Chronic symptoms: Fatigue, weakness. sleepiness, liaht headedness, numb
and tioalioa limbs, nausea, eye and skin irritation. vertigo, choking (2}
First Aid: Inhalation; artificial respiration; Ingestion; get medical
attention immediately; Eye contact: irrigate immediately; Skin contact:
soap and water wash immediately
•
Chemical Name: Methvlene Chloride
III. HAZARDOUS CHARACTERISTICS
Refeience
A. Combustibility Yes ....X No
Toxic by-products
B. Flammability LEL _..1_..2_,.% __ _
•
UEL --1~9-% __ _
c. Reactivity Hazard incompatible with strong oxidizers
and caustics, chemically active metals such as Al or Mg powders,
sodium, potassium,
D. Corrosivity Hazard
Neutralizing agent:
E. Radioactive Hazard
Background
Alpha particles
Beta particles
Gamma radiation
IV. REFERENCES
yes/no
yes/no
yes/no
yes/no
yes/no
pH:
(1) The Merck Index, 11th Edition, 1989
Exposure Rate
<2> Pocket Guide to Chemical Hazards, NIOSH, 1990
(3) Threshold Limit Values and Biological Exposure
Indices for 1997, ACGIH
(4) 29 CFR 1910 1052
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Ethyl Benzene
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula
Natural Physical State at 25oC liquid
Vapor Pressure 10 mm Hg at 79oF
Melting Point ~oE/oC Boiling Point moE/oC
Flash Point (open or closed cup) 59-64oC/oE
Solubility - H20 0.01%
other miscible with usual organic
solvents
1. 2
1. 2
2
1. 2
2
Physical Features: (odor, color, etc.)
flammable liquid with an aromatic odor. IP
colorless.
= 8,76 ev
Relative Response OVA= 100%
II. TOXICOLOGICAL DATA
Standards: 100 ppm (3) TLV
2000 ppm (2) IDLH
100 ppm (4) PEL
Routes of Exposure:
contact
Inhalation. Ingestion. Skin/Eye
Acute/Chronic Symptoms:Irritation of the eyes and mucus
membranes. headache. skin problems. sleepiness. coma (2)
First Aid: Inhalation: artificial respiration; Ingestion:
get medical attention immediately; Eye contact: irrigate
immediately; Skin contact: soap and water wash immediately
•
Chemical Name: Ethyl Benzene
III. HAZARDOUS CHARACTERISTICS
Reference
A. Combustibility Yes x_ No
Toxic by-products none known
B. Flammability LEL .LJl..%. UEL 6, 7%
c. Reactivity Hazard Strong oxidizers
•
D. Corrosivity Hazard yes/=. pH: --
Neutralizing agent:
E. Radioactive Hazard Exposure Rate
Background yes/=.
Alpha particles yes/=.
Beta particles yes/=.
Gamma radiation yes/=.
IV. REFERENCES
Cl) The Merck Index. 11th Edition. 1989
(2) Pocket Guide to Chemical Hazards. NIOSH 1990
13) Threshold Limit Values and Biological Exposure
Indices for 1997 ACGIH.
14) 29 CFR 1910,1000.
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Trichloroethylene
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula ~C~2~HuC~1~3~-----------
Natural Physical State at 2s0 c liquid
Vapor Pressure -~5~8'---mm Hg at 20°c
Melting Point =-2929c._ __ 0 £F/°C Boiling Point
Flash Point (open or closed cup) 32°C/°F
Solubility - H
20 0.1% at 77°F
Other Ether. alcohol. chloroform
Physical Features: (odor. color. etc.) Colorless
(unless dyed) with a sweet odor like chloroform lP
OVA Relative Response -70%
liquid
9.45 ev (2)
II. TOXICOLOGICAL DATA
Standards: 50 ppm (4) TLV
IDLH
potential
human
Routes of Exposure:
contact (2)
100 ppm (5) PEL carcinogen(2)
Inhalation. ingestion. skin and/or eye
Acute/Chronic Symptoms: Acute: Headache. vertigo. visual
disturbance. tremors.
drowsiness. nausea. vomiting. eye irritation. dermititis.
irregular heartbeat.
skin irritation; chronic: carcinogenic (2)
First Aid: Inhalation: artificial respiration; Ingestion: get
medical attention immediately; Eye contact: irrigate
immediately; Skin contact: soap and water wash immediately
• •
Chemical Name: Trichloreothylene
III. HAZARDOUS CHARACTERISTICS Reference
A.
B.
Combustibility
Toxic by-products
Flammability
Yes~ No -
LEL 12.5% UEL __ 9_0_% __ =
c. Reactivity Hazard Incompatible with strong caustics:
when acidic reacts with aluminum. chemically active metals.
barium. lithium. sodium. magnesium. titanium.
D. Corrosivity Hazard yes/no pH:
Neutralizing agent:
E. Radioactive Hazard Exposure Rate
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCES
(1) The Merck Index. 11th Edition. 1989
(2) Pocket Guide to Chemical Hazards. NIOSH. 1990
(3) Chemical and Engineering News. December 12. 1988,
(4) Threshold Limit Values and Biological Exposure
Indices for 1997 ACGIH
(5) 29 CFR 1910.1000
co1111care
NETWORK,INC.
WORKERS' COMPENSATION MEDICAL AUTHORIZATION
j Name of Employee/Patient: Last
/ Date of Iniurv:
/ Name of Employer/Company:
Employer Authorization:
First
/ Social Securirv Number:
STATE OF NORTH CAROLINA DEHNR
Doctor To Be Seen:
Emplover:
Emplovee:
Complete this form, and give it to the injured employee before a doctor is seen.
Show this form to the doctor.
Sec. No. 4.0
Rev. N,,. 4
Dote: 8-20-'
Page 2 of 2
Phvsician: When a referral is necessary -use CompCare Physicians and call 1-800-366-!5 ! ! , to let
the state agency claims represent.a.rive know that the patient is being referred.
SEND BILL DIRECTLY TO KEY RISK MANAGEMENT SERVICES, INC.
;:·.RA
NCDENR
J.-.MES 8. HUNT JR.
GoVCRNOR
•
Mr. Mitchell T. Arnold
Environmental Health Supervisor
Granville-\/ ancc District
l 15 Emergency Road
Henderson, NC 27536
NORTH ~ROLJNA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WASTE MANAGEMENT
May 22, 1998
RE: Site Inspection: On-site Reconnaissance
Cristex Drum Site
NCD00 1606250
Dear Mr. Arnold:
David Lilley of the NC Superfund Section spoke with Anita Paul of vour office today to
notify you that the NC Supcrfund Section will conduct a site reconnaissance of the subject site
located in Granville County, North Carolina. The reecnnaissancc will be conducted on June 1, 1998
by Donna Wilson of the NC Superfund Section.
The purpose of the reecnnaissance is to determine if the site poses a hazard to public health
or the environment because ofreleascs of contaminants to soil, surface water, groundwater, or air.
You may want to have your representative meet the reconnaissance team at the site. If so, please
contact Donna Wilson at [phone], ext 317 and she will coordinate a meeting.
If the reconnaissance indicates the need for future study of the site, we will contact your
office to advise. If you have any questions, please don't hesitate lo call David Lilley or me al (919)
733-280 I.
Enclosures
cc: Phil Prete
Doug Holyfield
Pal Williamson
Scott Ross
David LillC\·
Donna Keith
Sincerely,
~&~~/
Pat DeRosa, Head
Site Evaluation and Removal Branch
NC Superfund Section
401 OBERL.IN ROAD, SUITE 150, RALEIGH, NC 27605
F'HONE 919-733-4996 FAX [phone]
AN EQUAL OPPORTUNITY/ AFFIRMATIVE ACTION EMPLOYER· 50% RECYCLED/I 0% POST-CONSUMER PAPER
· Federal · ·
9Trip Notification & Authoriza.
Today's Date: 5 -Z{-78
• U:;c IJ]:1cl: !nl: or Tn.cw:i1cr onl~·St<1rf 10 fill ou; fi:-:.: ~ blod:s only:
Site Trip.
Date of Trip: .Ju/J.e_ I /"19/,'
Jr trip d~te changed or cancclJE:d note below:
Trip Date Changed To: ____ Cancelled:
NCD#: Oo I £06 z.so Site Name: Cn·s/c>c b,'-' "-Stf12.
City: O'xJv,cf County: <Jt.rci/\ 1,,'lle_
Name of Hotel (Overnight Trip): __ ,.,v,_/4~-----Hotel Telephone Number: ( ) _ -__ _ I
Project Team Leader: 0)fiM..-(/J/fx,/1
Attach To Notification Form: 1 copy each:
Submit to the
Industrial Hygienist
Authorized b}':
·-----------'---------
Preliminary Assessment Form (First page only)
Site Map
PA Transmittal Letter
(l'lc.!Sc lis: approp:-ia1c County Health Dcpanmcn: contact p:rson to call to advise of trip;) . .-r · .•· ,.., r . , . . EnvironmenI2.l Supervisor Oi He2.hh Director 10 call: /; 1,--f/_/.;, // ~i,> n<'ij Title:
c /1 l fl..:cc.14'i s;_,,, -,,e. ;/, ·x :-
(Note if Dr.. M.P., etc.)
Telephone Number: (i/7)[13-c)('.QX'
Notes: Health Dep2nment Official Contacted:
Back Uo Letter Reouired: Yes ./ /. , No
Nole: Si:::nctl original 10 Dat:J M:.in:.i;..:::~
•
SITE HEALTH AND SAFETY PLAN
A. General Information
•
Site Name Cristex ID# NCO 001 606 250
Location Corner of Industrial Dr, and Pine Tree
Rd, Oxford, Granville County, NC
Proposed Date of Investigation MM~a~r~c"h_._9~·~1~9~9~8~-------
Date of Briefing ~M~aur~c~h~~6~,~1~9~9~8,_ _____________ _
Date of Debriefing ~M~aur~c"h_._l~P~-~i~g~g~s,_ ____________ _
Nature of Visit (check one): On-Site Reconnaissance
Off-Site Reconnaissance
Sampling
Sampling Overview
Remediation Overview
x
Health Department Official contacted Ms, Judith Preddy for Mitchell Arnold
Date of contact February 19, 1998
Site Investigation Team: All site personnel have read the Site Health and
Safety Plan and are familiar with its provisions.
Personnel Responsibilities Signature
Team 1 Donna Wilson
Team 1 Jeanette Stanley
team leader, recon
reconnaissance
Team l BB.Yid HattjeGfe reconnaissance
Team 2
Reviewed By:
Plan Preparation: /Jl (} ,I
Prepared By: David Lilley. Industrial Hygiene Consultant '{).,.J'J'·
.,J_.a.,c.,k.__.B,;u .. t,._,.1.,,e,.r~,'--'s.,u._p.,e ..... r_.f_.u"n..,,d._,s.,e.,_c,._..t_.i..,o"-nl......lc"'h"-1,"-· e,....f ___ ~ n""""""'~,I
• •
B. SITE/WASTE CHARACTERISTICS
Waste Type(s) _x__Liquid _x__solid ___ Sludge ___ Gas _x__vapor
Characteristics ___ corrosive _x__rgnitable ___ Radioactive
_x..__volatile _x__Toxic ___ Reactive ___ Other
List Known or Suspected Hazards (physical, chemical biological or
radioactive) on Site and their toxicological effects.· Also, if known, list
chemical amounts
HAZARD
Tetrachloroethene
Toluene
Xylene
Barium
Chromium
Methylene Chloride
Ethvlbenzene
Trichloroethvlene
EXPOSURE
WARNING PROPERTIES LIMIT
Odor Threshold (OT) -4,68 -50 ppm
OT -0,17 -40 ppm
OT= 0,05 -200 ppm
OT no data
OT -no data
OT no data
OT-25-30 ppm (can adapt t9 odor)
OT -0,25 -200 ppm
OT -0,2 -400 ppm
UNDERGROUND UTILITIES CHECKLIST
25 ppm
50 QPID
100 ggm
0.5 mg/m3
0.1 mg/m3
0.05 mg/m'
25 ppm
100 ppm
50 ppm
Util·ity Locator/Contact Person Phone# Date of Location
Power
Telephone
Gas
Water
Sewer
Call made by:
2
• •
ID# NCO 001 606 250
Facility Description: Size unknown Buildings unknown
Disposal Methods Being Investigated ~e~uur~i~e~d.._d,.....r~uwmlia~,~-------------
Unusual Features on Site (dike integrity, power lines, terrain, etc.):
History of the Site: The site was a former textile mill and the drums were
discovered while conducting a site visit to JFD Electronics,
C. HAZARD EVALUATION
The site can be toured in level D protection, No samolina will be
conducted at this time. steel toed work boots will be worn while touring
D. WORK PLAN INSTRUCTION
Map or Sketch Attached? .v~e~s~---
Perimeter Identified? -o~o'-----
Command Post Identified? ~o~o'-----
Zones of Contamination Identified? _n_o'-----
Personal Protective Equipment/Level of Protection:
Modifications
3
___ c
•
Surveillance Equipment:
HNU
OVA
Explosimeter
Decontamination Procedures
•
ID# NCO 001 606 250
Detector Tubes and Pumps
02 Meter
Radiation Monitor
_____ Level C Respirator wash, respirator removal, suit wash (if needed),
suit removal, boot wash, boot removal and glove removal.
-~~ __ Level D Boot wash and rinse and boot removal, suit removal, glove
and goggle removal.
Modifications Dispose of trash properly, on site if possible,
Work Schedule/Visit Objectives The purpose of this visit is to determine
if the site poses a threat to the public health or environment because of
releases of contaminants to soil, surface water, groundwater, or air,
No samolina will be conducted at this time, samolina mav take place on a
EMERGENCY PRECAUTIONS
Route of Exposure
Inhalation
I nae st ion
4
First Aid
irrigate immediately
soap and water wash
fresh air and artificial respiration
get medical attention immediately
• •
ID# NCO 001 606 250
Location of Nearest Phone: unknown (nearby residences/businesses?)
Hospital (Address and Phone Number)
Granville Medical center, College St, Extention, PO Box 947, Oxford, NC
I 919) 693 5115 can handle chemically contaminated patients
Emergency Transportation Systems {Phone Numbers)
Fire 1919) 690-3000
Ambulance 1919) 690-3000
Rescue Squad 19191 690-3000
Emergency Route to Hospital Take the access road back to SR 1004, turn
riaht, and stay on SR 1004 to Route 15/158/96 and turn left, Travel north
approximately 1 mile, the hospital will be on the right,
PREVAILING WEATHER CONDITIONS AND FORECAST Partly cloudy with a chance of
rain, high in the low 60s,
EQUIPMENT CHECKLIST
___ Air purifying respirator
___ Cartridges for respirator
___ Eye Wash Unit
-~X-First Aid Kit
X 3 gal. Deionized H20
_ _.._ Rain suit
___ HNU -~-Gloves (PE/.PYC/nitrile/cloth)
___ OVA X Boots/Boot Covers
___ Explosimeter
___ Radiation Monitor
-~x-Decontamination
-~x_ Coveralls (tvvek/saranex) -~x-Eye Protection (goggles/shield)
-~X-Hard Hat
Materials
ASHEVILLE
704-255-4490
CHARLOTTE
704-379-5827
DURHAM
1-800-672-1697
GREENSBORO
919-379-4105
safeform.323a
------·========~;:----~------' Poison control Center -State Coordinator
eke/University Medical Center
Telephone: [phone]
Box 3024 _.,
Durham, NC 27710
Western NC Poison HENDERSONVILLE
Control Center 704-693-6522
Memorial Mission Hosp. Ext. 555,556
509 Biltmore Ave. 28801
Mercy Hospital
2001 Vail Ave, 28207
Duke Univ. Med. Center
Box 3007, 2 7710
Moses Cone Hospital
1200 N. Elm St. 27420
HICKORY
704-322-6649
JACKSONVILLE
919-577-2555
WILMINGTON
919-343-7046
5
Margaret R. Pardee
Memorial Hospital
Fleming St., 28739
Catawba Mem. Hosp.
Fairgrove Chur. Rd 28601
Onslow Mem. Hospital
Western Blvd. 28540
New Hanover Mem. Hospital
2131 S. 17th St. 28401
:CFC Pesticide
Jlspo,sal
,jCD 986 18D 883
· •019 ~;:-°:-4mM~~a-'--I~~~~
17'30·
-• I I \ \\,:.::· ));1(0!_---; (~:,,, -,,) 1o\\\. ',
•018 \ \\ ! ) ( ~'
1 ~,.~ 2· ) ) \ ,'• I i -.,___, .... _,, \ / \\ ---~ . ..,-.,
~<,OJ\ ) -_\_ •.\.'~7 ~r,1--...
__ ,,. . ~-~ 1 eJ \, -~ , \ {\, -~:o~
.::-:----.., /• I \ ', 1 1' 111 : -.· -. : I ,, , ' t) ,,_ -~:: ) i~~-/4~' \\✓-:-~~---, \ i.':l...,-\ )\ / ' \ \' ,._ I , • I
., .'.
·-..-~:~;,
• •
TO BE COMPLETED BY PROJECT MANAGER
PROJECT MANAGER: Donna Wilson PROJECT: ~C~rji~sut~e~x._ ______ _
INVESTIGATION DATE: March 9. 1998
RECONNAISSANCE ____..lL_ SAMPLING VISIT __ REMEDIATION/SAMPLING OVERVIEW
Respirator Worn By Approximate Time in Respirator
Air Monitoring Data (Include Calibration Reading)
HNU:
OVA:
Explosimeter:
Radiation Meter:
Were there any injuries? If yes, explain: ______________ _
If the maximum personal protective equipment as outlined in the Hazard
Evaluation Section was not used, please justify:
Visitors Present Organization Represented
Signature
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Perchloroethylene
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula
Natural Physical State at 25oc liguid
Vapor Pressure __ 1~4 __ mm Hg at 20oc
2
2
Melting Point --~2 __ oE/oC Boiling Point 250 oE/oC _2 __
Flash Point (open or closed cup) NIA oC/oF
Solubility - H20 0.015% 2
Other misc with alcohol. ether.
chloroform. benzene
Physical Features: (odor, color, etc.) colorless
liguid with an odor like ether or chloroform IP-9.32 ev
/2) OVA Relative Response -70%
II. TOXICOLOGICAL DATA
suspect human
standards: 25 ppml3)TLV 100 ppml4)PEL carcinogen /2)IDLH
Routes of Exposure: Inhalation. Ingestion. Skin and/or
Eye contact /2)
Acute/Chronic Symptoms: Irritation of eyes. nose. and
throat. nausea. flushed face and neck. vertigo. dizziness.
incoordination. headache. carcinogen 12)
First Aid: Inhalation: artificial respiration;
get medical attention immediately; Eye contact:
immediately; Skin contact: soap and water wash
immediately.
Ingestion:
irrigate
•
Chemical Name: Perchloroethylene
III. HAZARDOUS CHARACTERISTICS
Reference
A. Combustibility Yes
Toxic by-products
B. Flammability LEL none
No _x_
UEL
•
none
c. Reactivity Hazard Incompatible with
oxidizers. chemically active metals. such as
lithium. and beryllium & barium; caustic soda;
hydroxide. potash (2)
D. Corrosivity Hazard yes/no pH:
Neutralizing agent:
E. Radioactive Hazard Exposure Rate
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCES
1. The Merck Index. 11th Edition. 1989
_.2.._
2
strong
barium.
sodium
2. NIOSH Pocket Guide to Chemical Hazards. 1990
3. Threshold Limit Values and Biological Exposure
Indices for 1997 ACGIH.
4 • CFR 1910.1000.
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Toluene <Methyl benzene. toluol}
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula C7H8
Natural Physical State at 25°C liquid
Vapor Pressure __2_Q_ mm Hg at 20°c
Melting Point -95°F/0
~ Boiling Point
Flash Point (open or closed cupl 40 ll0.6°F/°~ OC/°E.
1.2.3.4
1.2.3.4
1,3,4
1.2.3.4
Solubility -H,O slightly soluble 1.3.4
other miscible with alcohol. 1.3.4
chloroform. ether. acetone.
glacial acetic acid. carbon
disulfide
Physical Features: /odor. color. etc.} colorless
liquid with an aromatic odor. IP 0.02 ev. /3} derived
from coal tar oil or petroleum Relative response on
II. TOXICOLOGICAL DATA
Standards: 50 ppm 15} TLV
100 ppm /6} PEL 2000 ppm /4} IDLH
Routes of Exposure:
contact. eye contact
inhalation; ingestion. skin
Acute/Chronic Symptoms:
headache. lassitude. and
Narcotic in high concentrations.
nausea, Chronic: anemia and
dermatitis, 12}
First Aid: Inhalation: artificial respiration;
get medical attention immediately; Eye contact:
immediately; Skin contact: soap and water wash
immediately
Ingestion:
irrigate
•
Chemical Name: aT~o~l~u=e~n~e~--------
III. HAZARDOUS CHARACTERISTICS
Reference
A. Combustibility Yes x_ No
Toxic by-products
B. Flammability LEL .J.....Ql UEL -~1~,~0~%-
C. Reactivity Hazard strong oxidizers
•
D. Corrosivity Hazard yes/filL pH: --
Neutralizing agent:
E. Radioactive Hazard Exposure Rate
Background yes/DQ
Alpha particles yes/DQ
Beta particles yes/DQ
Gamma radiation yes/DQ
IV. REFERENCES
Ill The Merck Index. 11th Edition. 1989
3
121 Documentation of the TLV. 4th Edition. 1980
13} NIOSH Pocket Guide for Chemical Hazards. 1990
14} NEPA. Protection Guide on Hazardous Materials.
Bth Edition. 1984
15} Threshold Limit Values and Biological Exposure
Indices for 1997
16} 29 CFR 1910.1000
4
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Xylene. o. M. & P (Dimethyl benzene)
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula ...J;8_H10 ______ _
Natural Physical State at 25°C liquid
Vapor Pressure l='-2_ mm Hg at 20°c
Melting Point 13-14°F/°C Boiling Point 137-140°F/°C _l...._
Flash Point (open or closed cup) 90/84/81°C/0 E
Solubility -H20 insoluble
Other soluble in alcohol, ether
and most other organic solvents.
Physical Features: (odor, color, etc.) colorless liquid with
aromatic/ benzene odor. common solvent for paints and coatings.
IP -B.5 ev. HNU relative response with 10.2 ev probe -11.3. OVA
relative response= 111 -116%
II. TOXICOLOGICAL DATA
Standards: 100 ppm (2l TLV
IDLH
100 ppm (3) PEL 1.000 ppm (4)
Routes of Exposure: Inhalation. Ingestion. Skin and/or Eye
contact
Acute/Chronic Symptoms: headache. fatigue. dizziness. lassitude.
narcotic effects in high concentrations (5.6l. Chronic effects not
well defined (ll.
First Aid: Inhalation: artificial respiration; Ingestion: get
medical attention immediately; Eye contact: irrigate immediately;
Skin contact: soap and water wash immediately.
•
Chemical Name: Xylene. o. M. & P
III. HAZARDOUS CHARACTERISTICS Reference
E.
A. Combustibility Yes _x No
Toxic by-products
B. Flammability LEL 1,4% UEL .h1..%_
c. Reactivity Hazard strong oxidizers
D. Corrosivity Hazard
Neutralizing agent:
Radioactive Hazard
Background yes/DQ
Alpha particles yes/DQ
Beta particles yes/DQ
Gamma radiation yes/DQ
yes/no pH:
Exposure Rate
IV. REFERENCES
(1) The Merck Index. 11th Edition. 1989.
•
1.2.3.4
(2) Threshold Limit Values and Biological Exposure
Indices for 1997
(3) 29 CFR 1910, 1000
(4) NIOSH Pocket Guide to chemical Hazards. 1990.
5) NFPA. Fire Protection Guide on Hazardous
Materials. sth Edition. 1984.
(6) Documentation of the TLV. 4th Edition. 1980
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Barium (soluble compounds)
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula
Natural Physical State at 25oC
depending on compound
properties vary
Vapor Pressure ----~ mm Hg at 20°c
Melting Point ___ °F/°C Boiling Point ___ °Fj°C
Flash Point (open or closed cup) _°C/°F
Solubility - H20 vary
Other
Physical Features: (odor, color, etc.)
depending on compound(2)
II. TOXICOLOGICAL DATA
Standards: 0.5 mg/m3(3) TLV 0.5 mg/m3(4l PEL
1.100 mg/m3/2l IDLH
vary
Routes of Exposure:
eye contact
Inhalation. Ingestion. skin and/or
Acute/Chronic Symptoms: Upper respiratory irritation. GI
irritation. muscle spasms. slow pulse. premature
contractions of the heart. extrasystoles. hypokalemia.
irritation of eyes. skin burns. (21
First Aid: Inhalation: artificial respiration; Ingestion:
get medical attention immediately; Eye contact: irrigate
immediately; Skin contact: soap and water wash
immediately.
•
Chemical Name: Barium
III. HAZARDOUS CHARACTERISTICS
Reference
A. Combustibility Yes No
Toxic by-products
•
depends on compound
B. Flammability LEL UEL
c. Reactivity Hazard depends on compound
D. Corrosivity Hazard yes/no pH:
Neutralizing agent:
E. Radioactive Hazard Exposure Rate
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCES
1. The Merck Index. 11th Edition. 1989
2. Pocket Guide to Chemical Hazards. NIOSH. 1990
3. Threshold Limit Values and Biological Indices
for 1997 ACGIH.
4. 29 CFR 1910.1000
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Chromium (YI). insoluble salts
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula varies with compound
Natural Physical State at 25°c solid
Vapor Pressure -~H~L~A~~ mm Hg at 20°c
Melting Point ---~"F/°C Boiling Point ----="F/°C
Flash Point (open or closed cup) ---=N~/=A~="C/°F
Solubility -H20 not soluble in water
Other
Physical Features: (odor, color, etc.) Properties vary
depending upon specific compound. compounds include: zinc
chromate. lead chromate. calcium chromate. etc.
II. TOXICOLOGICAL DATA
Standards: 0.01 mg/m3 (2) TLV 0.5mg/m3 (4) PEL 500 mg/m3 (3) IDLH
Routes of Exposure: Inhalation and ingestion
Acute/Chronic Symptoms: Chronic: fibrosis of the lung and
epidemiological studies have shown increased incidence of lung
cancer among workers in the manufacture of chrome pigments
First Aid; Inhalation: artificial respiration: Ingestion: get
medical attention immediately; Eye contact: irrigate
immediately; Skin contact: soap and water wash immediately
•
Chemical Name: Chromium (VIl. insoluble salts
III. HAZARDOUS CHARACTERISTICS Reference
A. Combustibility Yes _ No~
Toxic by-products
B. Flammability LEL NIA UEL
c. Reactivity Hazard strong oxidizers
D. Corrosivity Hazard yes/no pH:
Neutralizing agent:
E. Radioactive Hazard
Background
Alpha particles
Beta particles
Gamma radiation
IV. REFERENCES
yes/no
yes/no
yes/no
yes/no
Exposure Rate
1. The Merck Index. 11th Edition. 1989.
2. Threshold Limit Values and Biological Exposure Indices
for 1997 ACGIH
3. Pocket Giude to Chemical Hazards. NIOSH. 1990
4, 29 CFR 1910.1000
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Lead. inorganic dusts
I. PHYSICAL/CHEMICAL PROPERTIES
Chemical Formula
Natural Physical State at 25°C solid
Vapor Pressure .JU.A mm Hg at 20°c
Reference
Melting Point 327.4°F/°C Boiling Point l.740°F/°C
Flash Point (open or closed cup) NJ.1,.°C/°F
Solubility - H20 .JU.A
Other~'+-"-~-----------
Physical Features: (odor, color, etc.) appearance and odor
vary depending upon specific compound.
II. TOXICOLOGICAL DATA
suspected or confermed human
Standards: .05 mg/m3 (2) TLV
N/A /4) IDLH
carcinogen
0.05 mg/m3 /3) PEL
Routes of Exposure:
contact(3)
inhalation. ingestion. eye contact. skin
Acute/Chronic symptoms:Acute; lassitude. pallor. constipation.
abdominal pain. gingival gum line. tremors. Target organs; GI
tract. CNS. kidneys. blood,<3)
First Aid: Inhalation; artificial respiration; Ingestion: get
medical attention immediately; Eye contact: irrigate immediately;
Skin contact: soap and water wash immediately
•
Chemical Name: Lead. inorganic dusts
III. HAZARDOUS CHARACTERISTICS
A. Combustibility Yes
Toxic by-products
B. Flammability
c. Reactivity Hazard
D. Corrosivity Hazard
Neutralizing agent:
No _x_
LEL N/A
None
yes/no
•
Reference
UEL __ _
pH: -
E. Radioactive Hazard Exposure Rate
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCES
Ill The Merck Index. 11th Edition. 1989
r2l Threshold Limit Values and Biological Exposure
Indices for 1997 ACGIH.
/3} 29 CFR 1910.1025
/4} Pocket Guide to Chemical Hazards. NIOSH. 1990.
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Methylene Chloride
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula CH2 C12 __________ _
Natural Physical State at 25°C __..l~i~q~u~i~d._ ___ _
Vapor Pressure 350 mm Hg at 20°c
Melting Point -139 °F/°C Boiling Point 104 °F/0c
Flash Point (open or closed cup) --~? ___ °C/°F
solubility -H2O soluble in SO parts water
Other misible with alcohols, ether,
Physical Features: (odor, color, etc.) Colorless liquid with a
chloroform-like odor (2) IP -11,35 ev, Relative response on
HNU -9,4, OVA Relative Response -100%
II. TOXICOLOGICAL DATA
Standards: so ppm/3) TLV 25 ppm/4) PEL
suspect human
carcinogen
IDLH
Routes of Exposure: Inhalation, ingestion, eye contact, skin contact
Acute/chronic Symptoms: Fatigue, weakness, sleepiness, light headedness, numb
and tinalina limbs, nausea, eve and skin irritation, vertigo, choking <2>
First Aid: Inhalation; artificial respiration: Ingestion; get medical
attention immediately: Eve contact; irrigate immediatelvi Skin contact;
soap and water wash immediately
•
Chemical Name: Methylene Chloride
III. HAZARDOUS CHARACTERISTICS
Reference
A. Combustibility Yes _x No
Toxic by-products
B. Flammability LEL _..l_..2"'% __ _
•
UEL __ 1~9_% __ _
c. Reactivity Hazard incompatible with strong oxidizers
and caustics. chemically active metals such as Al or Ma powders,
sodium, potassium.
D. Corrosivity Hazard yes/no
Neutralizing agent:
E. Radioactive Hazard
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCES
pH:
(1) The Merck Index. 11th Edition, 1989
Exposure Rate
(2) Pocket Guide to Chemical Hazards, NIOSH, 1990
(3\ Threshold Limit Values and Biological Exposure
Indices for 1997, ACGIH
14) 29 CFR 1910 1052
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Ethyl Benzene
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula ~C~B-li~l~0~-----------
Natural Physical State at 25oC liguid
Vapor Pressure 10 mm Hg at 79oF
Melting Point =-1.lloE/oC Boiling Point 2J..l..oE/oC
Flash Point {open or closed cup) 59-64oC/oE
Solubility -H20 0.01%
other miscible with usual organic
solvents
1.2
1.2
1.2
Physical Features: (odor, color, etc.) colorless.
flammable liguid with an aromatic odor. IP -a.76 ev
Relative Response OVA= 100%
II. TOXICOLOGICAL DATA
Standards: 100 ppm (31 TLV
2000 ppm (21 IDLH
100 ppm (41 PEL
Routes of Exposure:
contact
Inhalation. Ingestion. skin/Eye
Acute/Chronic Symptoms:Irritation of the eyes and mucus
membranes. headache. skin problems. sleepiness. coma /2)
First Aid: Inhalation: artificial respiration; Ingestion:
get medical attention immediately; Eye contact: irrigate
immediately; skin contact: soap and water wash immediately
Chemical Name: Ethyl Benzene
III. HAZARDOUS CHARACTERISTICS
Reference
A. Combustibility Yes x_ No
Toxic by-products none known
B. Flammability LEL .LJll UEL 6.7%
c. Reactivity Hazard strong oxidizers
•
D. Corrosivity Hazard yes/DQ pH: --
E.
Neutralizing agent:
Radioactive Hazard Exposure Rate
Background yes/DQ
Alpha particles yes/DQ
Beta particles yes/DQ
Gamma radiation yes/DQ
IV. REFERENCES
(1) The Merck Index. 11th Edition. 1989
(2) Pocket Guide to Chemical Hazards. NIOSH 1990
2
(3) Threshold Limit Values and Biological Exposure
Indices for 1997 ACGIH.
(4) 29 CFR 1910.1000,
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Trichloroethylene
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula =C-2~li~C~1~3~----------~
Natural Physical State at 25°C liquid
Vapor Pressure 58 mm Hg at 20°c
Melting Point --~9~9 ___ °F~/°C Boiling Point -=1=8=9 __ 0 ~F/°C
Flash Point (open or closed cup) 32°C/°F
Solubility - H
20 0.1% at 77°F
Other Ether. alcohol. chloroform
Physical Features: (odor, color, etc.) Colorless liquid
<unless dyed) with a sweet odor like chloroform lP -9,45 ev /2)
OVA Relative Response -70%
potential
human
II. TOXICOLOGICAL DATA
Standards: 50 ppm (4} TLV
IDLH
100 ppm C5l PEL carcinogen/2)
Routes of Exposure:
contact C2l
Inhalation. ingestion. skin and/or eye
Acute/Chronic Symptoms: Acute: Headache. vertigo. visual
disturbance. tremors.
drowsiness. nausea. vomiting. eye irritation. dermititis.
irregular heartbeat.
skin irritation; chronic; carcinogenic r2l
First Aid: Inhalation; artificial respiration; Ingestion; get
medical attention immediately; Eye contact; irrigate
immediately; Skin contact; soap and water wash immediately
• •
Chemical Name: Trichloreothylene
III. HAZARDOUS CHARACTERISTICS Reference
A.
B.
Combustibility
Toxic by-products
Flammability
Yes~ No
LEL 12.5% UEL 90%
c. Reactivity Hazard Incompatible with strong caustics:
when acidic reacts with aluminum. chemically active metals.
barium. lithium. sodium. magnesium. titanium,
D. Corrosivity Hazard yes/no pH:
Neutralizing agent:
E. Radioactive Hazard Exposure Rate
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCES
(1) The Merck Index. 11th Edition. 1989
(2) Pocket Guide to Chemical Hazards. NIOSH. 1990
(3) Chemical and Engineering News. December 12. 1988,
(4) Threshold Limit values and Biological Exposure
Indices for 1997 ACGIH
(5) 29 CFR 1910,1000
COIIHIC3n!
NETWORK,INC.
WORKERS' COMPENSATION MEDICAL AUTHORIZATION I Name of Employee/Patient: Last
I Date ofiniurv:
I Name of Employer/Company:
Employer Authorization:
First
I Social Securitv Number:
STATE OF NORTH CAROLINA DEHNR
Doctor To Be Seen:
Emplover:
Emplovee:
Complete this fonn, and give it to the injured employee before a doctor is seen.
Show this fonn to the doctor.
Sec. No. 4.0
Rev. N.o. 4
Date: 8-20-9
Page 2 of 2
Physician: When a referral is necessary -use CompCare Physicians and call 1-800-366-1511, to let the state agency claims representative know that the patient is being referred.
SEN"D BILL DIRECTLY TO KEY RISK MANAGEMENT SERVICES, INC.
• FILE COPl
Mr. Mitchell T. Arnold
Environmental Health Supervisor
Granville-Vance District
I I 5 Emergency Road
Henderson, NC 27536
• NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WASTE MANAGEMENT
February 19, 1998
RE: Preliminary Assessment: On-Site Reconnaissance
Cristex Drum Site, NC0001606250
Dear Mr. Arnold:
David Lilley of the NC Superfund Section spoke with Ms. Judith Preddy of your office
today to notify you that the NC Superfund Section will conduct a site reconnaissance of the subject
site located in Ganville County, North Carolina. The reconnaissance will be conducted on March
9, 1998 by Donna Wilson of the NC Superfund Section.
The purpose of the reconnaissance is to determine if the site poses a hazard to public health
or the environment because of releases of contaminants to soil, surface water, groundwater, or air.
The reconnaissance team will locate all nearby water supplies (surface and groundwater, community
and private) and any close sensitive environments, schools, and day care centers.
This reconnaissance is not an emergency situation but is a normal step in the evaluation of
all uncontrolled and unregulated potential hazardous waste sites in North Carolina. You may want
to have your representative meet the reconnaissance team at the site. If so, please contact Donna
Wilson at [phone], ei,,:t. 317 and she will coordinate a meeting. I am enclosing background
data on the site for your information.
If the reconnaissance indicates the need for future study of the site, we will contact your
office to advise. If you have any questions, please don't hesitate to call David Lilley or me at (919)
733-2801.
Enclosures
cc: Phil Prete
Doug Holyfield
Pat Williamson
Scott Ross
David Lilley
Donna Keith
I
Sincerely,
Pat DeRosa, Head
Site Evaluation and Removal Branch
NC Superfund Section
401 OBERLIN ROAD, SUITE ISO, RALEIGH, NC 27605
PHONE 919·733-4996 FAX [phone]
AN EQUAL OPPORTUNITY/ AFFIRMATIVE ACTION EMPLOYER· 50% RECYCLED/! 0% POST-CONSUMER PAPER
•
SITE HEALTH AND SAFETY PLAN
A. General Information
Site Name Criatex ID# NCO 001 606 250
Location corner of Industrial Dr, and Pine Tree
Rd, Oxford, Granville County, NC
Proposed Date of Investigation -1~/~2~1~/~9~7'-----------
Date of Briefing
Date of Debriefing
Nature of Visit (check one): on-Site Reconnaissance
Off-Site Reconnaissance
Sampling
Sampling Overview
Remediation Overview x
Health Department Official Contacted ~Mwiut~cuh~e~l~l~A~r~nuo~l~d~-----------
Date of Contact KJ~a~nuUuaMr~y.__.1~2~-~lu9~9~2~----------------------
Site Investigation Team: All site personnel have read the Site Health and
Safety Plan and are familiar with its provisions.
Personnel
Team 1 Jeanette Stanley
Team l
Team 2
Team 2
Responsibilities Signature
overview
Plan Preparation: J/)_ J
Prepared By: David Lilley. Industrial Hygiene consultantzVJ £
Reviewed By: Jack Butler, Superfuod Section Chief
•
B. SITE/WASTE CHARACTERISTICS
Waste Type(s) ___ Liquid ___ Solid ___ Sludge ___ Gas ___ Vapor
Characteristics ___ Corrosive ___ Ignitable ___ Radioactive
___ Volatile ___ Toxic ___ Reactive ___ Other
List Known or Suspected Hazards (physical, chemical biological or
radioactive) on Site and their toxicological effects.
chemical amounts
HAZARD
unknown
Utility
Power
.Telephone
Gas
Water
Sewer
Call made by:
WARNING PROPERTIES
UNDERGROUND UTILITIES CHECKLIST
Locator/contact Person Phone#
2
Also, if known, list
EXPOSURE
LIMIT
Date of Location
• •
ID# NCO 001 606 250
Facility Description: Size unknown Buildings unknown
Disposal Methods Being Investigated -B~u~r~i~e~d~d-r~u~m~s~-~-------------
Unusual Features on Site (dike integrity, power lines, terrain, etc.):
History of the Site: The site was a former textile mill and the drums were
discovered while conducting a site visit to JFD Electronics,
C. HAZARD EVALUATION
The site can be toured in level D protection, No sampling will be
conducted at this time, Steel toed work boots will be worn while touring
D. WORK PLAN INSTRUCTION
Map or Sketch Attached? ~y~e~s~---
Perimeter Identified? ~o~o'-----
Command Post Identified? ~o~o'-----
Zones of Contamination Identified? ~o~o._ ___ _
Personal Protective Equipment/Level of Protection: ___ c,
Modifications
3
ID# NCO 001 606 250
X D
Surveillance Equipment:
_____ HNU ______ Detector Tubes and Pumps
•
_____ OVA
______ Exploeimeter
Decontamination Procedures
•
02 Meter
______ Radiation Monitor
----~Level C Respirator wash, respirator removal, suit wash (if needed),
suit removal, boot wash, boot removal and glove removal.
-~~-_.Level D Boot wash and rinse and boot removal, suit removal, glove
and goggle removal.
Modifications Dispose of trash orooerlv, on-site if possible,
work Schedule/Visit Objectives The purpose of this visit is to determine
if the site poses a threat to the public health or environment because of
releases of contaminants to soil, surface water, arouodwater, or air,
No samolino will be conducted at this time, sampling may take place on a
EMERGENCY PRECAUTIONS
Route of Exposure
Inhalation
Inaestion
4
First Aid
irrigate immediately
soap and water wash
fresh air and artificial respiration
get medical attention immediately
ID# NCO 001 606 250
Location of Nearest Phone: unknown (nearby residences/businesses?)
• •
Hospital (Address and Phone Number)
Granville Medical center, College St, Extention, PO Box 947, Oxford, NC
1919) 693 5115 can handle chemically contaminated patients
Emergency Transportation Systems (Phone Numbers)
Fire 1919) 690 3000
Ambulance 1919) 690-3000
Rescue Squad 1919) 690-3000
Emergency Route to Hospital Take the acceas road back to SR 1004, turn
right, and stay on SR 1004 to Route 15/158/96 and turn left, Travel north
approximately 1 mile, the hospital will be on the right,
PREVAILING WEATHER CONDITIONS AND FORECAST ________________ _
EQUIPMENT CHECKLIST
___ Air purifying respirator
Cartridges for respirator
Eye Wash Unit
x x
x
First Aid Kit
3 gal. Deionized H20
Rain suit
HNU
___ OVA
x
x
Gloves (PE/~/nitrile/cloth)
Boots/Boot Covers
x
Explosimeter
Radiation Monitor
Decontamination
x x
coveralls (tyvek/saranex)
Eye Protection (goggles/shield)
Hard Hat
Materials
Poison control center State Coordinator
Duke Un~versity Medical Center
Telephone: [phone]
ASHEVILLE
704-255-4490
CHARLOTTE
704-379-5827
Box 3024
Durham, NC 27710
Western NC Poison HENDERSONVILLE
Control Center 704-693-6522
Memorial Mission Hosp. Ext. 555,556
509 Biltmore Ave. 28801
Mercy Hospital
2001 Vail Ave, 28207
HICKORY
704-322-6649
~ . ..-------Duke "'t·ni V. Med. Cente~JACKSONVILLE
1-800-672-1697 Box 3007, 27710 919-577-2555
GREENSBORO
919-379-4105
safeform.323
Moses Cone Hospital
1200 N. Elm St. 27420
WILMINGTON
919-343-7046
5
Margaret R. Pardee
Memorial Hospital
Fleming st., 28739
Catawba Mem. Hosp.
Fairgrove Chur. Rd 28601
Onslow Mem. Hospital
Western Blvd. 28540
New Hanover Mem. Hospital
2131 S. 17th st. 28401
CCFC Pesticide
Disposal
NCO 986
• •
TO BE COMPLETED BY PROJECT MANAGER
PROJECT MANAGER: Jeanette Stanley PROJECT: ~G~c~i~s~t~e-x~-------
INVESTIGATION DATE: .l~/~2~1~{~9~7 ______ _
RECONNAISSANCE SAMPLING VISIT ___ REMEDIATION/SAMPLING OVERVIEW __x__
Respirator Worn By Approximate Time in Respirator
Air Monitoring Data (Include Calibration Reading)
HNU:
OVA:
Explosimeter:
Radiation Meter:
Were there any injuries? If yes, explain: ______________ _
If the maximum personal protective equipment as outlined in the Hazard
Evaluation Section was not used, please justify:
Visitors Present Organization Represented
Signature
;
Prepared by: LV,11/A,., /JJ1 {Sv't\
· U:-c Ill:.icl.: Ink or Typewriter only-S1,.1ff 10 fill out first~ blocks only.
Site Trip-
Date of Trip: ---'3::.. __ a,__1-_,_q_,.f, _______ _
If trip date changed or cancelled note below:
Trip Date Changed To: ____ Cancelled:
NCD#: _rv_c_o_· _00_·~L~"'-o~t_2-_su~
City: Qx{iyd
Reason for Trip:
.Site Name: Cr, sf::y if</IVl Sire
County: ('/rtlflv,)le
Today's Date: 2 -19 -18
Name of Hotel (Overnight Trip): ________ Hotel Telephone Number: ( ) _ -__ _
Project Team Leader: J)Cl\/\th.-(,,(J 1' (~I'\.
Assistants: je~ !\/'±h,, Sbrf\ leo/ , ________________ _
Attach To Notification Form: 1 copy each:
Submit to the
Industrial Hygienist
Preliminary Assessment Form (First page only)
Site Map
PA Transmittal Letter
(Please list appropriate County Health Dcpanmcnt contact pcr..on 10 call to advise of trip)
Environmental Supervisor or Health Director to call: ;7] ;./-d.eJ( T-.L/rf\Q(j
Notes:
(Note if Dr., M.l'., etc.)
Telephone Number: A19)~'1'.>-~ 'il'~
Health Department Official Contacte;l-<-/)JS-. Ju J,;-lf: Pre,117
Back Up Letter Required: Yes _[L No __
/1J%/;erl!Jis. P«~ -& ltv-ffel'c~!/ <11'."\
Note: Si:,icd original to Data Mani:l;!Cr
·, . ..i&. Federal
'IP,ip Notification & Authorizatiof
•
Site Trip
Date of Trip: / /21 /q----z
If trip date cha4d ;cancelled note below:
Trip Date Changed To: _____ Cancelled:
NC D #: ,_,N""C.-'O--"'-o-"0_.,/,--,.,/,'-"0'-'(,_1 _,_;),.___.'.,_,,() Site Name: Cn-J ~ 'x
/) vk q,/ County: Cn10,u)le t; /t,q; I "'7
City:
Today's Date: / /;, /tj7 r1
Name of Hotel (Overnight Trip): ---~Nc......,/~l~t' ___ Hotel Telephone Number: ( ) _ -__ _
I
Authorized by:
" Industrial Hygicnis
Project Team Leader: ~ n eff-c, 5-k J/J/ iv;
Assistants:
Attach To Notification Form: 1 copy each:
Submit to the
Industrial Hygienist
Preliminary Assessment Form (First page only)
Site Map
PA Transmittal Letter
(!'lease hsi appmpria<c County l!callh Dcpartmcn<con<ac< pcr.;on lo call to adv;sc of <rip) . ·. / ! &/1-v, Jka !/1,_
Environmental Supervisor or Health Director to call: JD.r r;fJ,lde// 4-,.c,/c{__ Title: 5'~c11 .,.,.,-
Notes:
(No1c if Dr., M.P., etc.) _ ~~B"'S
Telephone Number: (ql"I )6'1'3-~ J Lf /
Health Department Official Contacted: /fl,fdef / .1/rn.,J/
Back Up Letter Required: Yes __ No fr--
l1J»J;'eJ /}J,,, 4co,_,/) <>1-\. /-17-1? (Ol.3t-}
Note: Sij!ncd original to Data Manai,:cr