NC0001606250_19990630_Cristex Drum_FRBCERCLA PA SI_Integrated PA SI) Volume III - References 13 - 18-OCR

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STATE OF
NORTH CAROLINA
Department of Environment
and fVaJural Resources
Division of Waste Management
Super:fund Section
INTEGRATED PRELIMINARY ASSESSMENT/SITE INSPECTION (PA/SI ' . VOLUME Ill REFERENCES 13 THRU lB I
Cristex Drum Site
NCO 001 606 250
Oxford, Granville County, NC
Reference No. 06597
June 1999
Jeanette Stanley
Environmental Chemist
Dfrision of Waste Afanagement
S11pe1f11nd Section
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EPIC Roll: 27748 (278) Frame 132 #90052
\ December 27, 1965
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To:
From:
Subject:
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MEMOR'(\NDUM
File
Donna Wilson~
Environn1ental Engineer
1 North Carolina Superfund Section
Onsite reconnaissance
Cristex Drum Site
Oxford, Granville County
Date: March 18, 1998
i
Ref 14
On March 9, 1998, Jeannette Stanley Jnd !'conducted an onsite reconnaissance of
the above referenced facility. We arrived at th6 siie at approximately 12:55 and parked
near the back locked gate to the Cristex facility1• We walked along the outside (east of the
Cristex facility) of the fence back to the drum dispbsal site. Another road is adjacent to ' ,,
the Cristex facility on the east side that leads to' a fenced, locked area that contains
propane tanks. This area is most likely the pro~ert~, owned by Empire Gas.
The lagoon is northwest of the drum sit~. 1\wo outfalls from the Cristex facility
discharge water to the lagoon. One of the outfalls is a square concrete manhole that
receives water from a ditch on the Cristex propJrty l~nd transfers the water to a pipe in the
northwest direction. Photo #1 was taken at this'loc~tion. Photo #2 was taken of the
' ' lagoon looking north. The second outfall is located directly below the large vertical tanks
on the Cristex property and appears to receive Jati from a structure inside the Cristex
facility. Discharge from the pipe empties into a'sm1ll pool of water, which overflows
into a pipe that transfers the water under a berm _intd ',the lagoon. Photos #3, 4, and 5 were
taken of the second outfall. A large amount of]jriaA prevented us from walking around
the western edge of the lagoon. \ \
At 1 :25, we walked along the east side otthe lagoon. Along the length of eastern
side of the lagoon appears to be a former drainag1e ditch lined on both sides with pine
trees. The ditch ends at the back of the lagoon iii a i<etland area. Also along the eastern
side of the lagoon, and not far from the former dium\site, was a dirt berm about 4 to 5 feet
high and 30 feet long. Only briars and brush (no !tree~) were growing on the berm. This
area may need to be investigated to determine if fr al~o contains buried drums.
The outlet of the lagoon is a open concrete miinhole on the northern berm.
Discharge from the manhole enters the City of Ol)foril's sewer system. Photo #7 was
taken of the manhole. i \ ·
The area north of the lagoon is a wetland area. Photo #8 was taken of this
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location. Groundwater flow from the lagoon to surface water in this area is a probability.
Approximately 50 feet east of the lag1oori is a clearing that appears to be an old
lagoon or drying bed. The surface is exposed reU clay with very little vegetation and was
wet at the time of our visit. Run-off from th6 ar6a flowed northeast, and dried up before
entering a surface water body. Photo #9 was\tak~n of this location.
The drum disposal area was north and wdst of the fenced Empire Gas property.
Photos # 10 and 11 were taken of the area. Photd # 12 was taken of the Empire Gas
property. Photo #13 was taken from the druri1 dikposal area looking south between the
two fences. \ \
At approximately 3: 10, we met with ~lo I;Ierringsmith (919-690-8624), who
works for CVS. The back of the Cristex facility is now used by CVS drugstores for
warehouse storage. The front of the building
1
is n16t being used. We walked through the
warehouse to exit the back door. Within the building, the only signs ofliquid discharge
were what appeared to be covered floor drainJ. rA'the back of the property, a drainage
ditch transverses the back of the property. Di~chJrge from inside the building appears to
have at one time entered the drainage ditch thfouJh a pipe under a concrete pad at the
northeast corner of the building. The drainagJ dit~h carries run-off under the facility
road to the lagoon manhole. \ \
There appears to be an underground storage tank area in the back of the facility
between the road and the drainage ditch. Seve1ral pipes were in the ground and there is a
large concrete pad containing gas pipes and prbssure valves surrounded by protective
poles. \ \
The two large vertical tanks are present• at the back of the facility.
At approximately 3:30, we left the site.\
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LEONHARDT
ENVIRONMENTAL
January 22, 1999
· State of North Carolina
Division of Waste Management
401 Oberlin Road
Suite 150
Raleigh, North Carolina 27605
Attention: Donna J. Wilson
Subject: Cristex Site
Oxford, North Carolina
Dear Ms. Wilson:
Ref 15
3208 Twin Leaf Drive
Raleigh, North Carolina 27613
[phone]
FAX [phone]Jl2
RECEIVED
JAN 26 1999
SUPERFUND SECTIC'W
/;s we have discussed, Mr. George Christensen, owner of the Cristex site, at your request,
suspended all environmentally related activities at his sit~ in Oxford, North Carolina, pending the
completion of your agency'~ investigation into the possible sources of nearby groundwater
~ontamination. As we understand it, the portion ofyout investigation dealing with the Cristex site
has been completed. It is our intention to now resume dctivities at the site which will include the
closure of the former wastewater treatment lagoon.
We intend to begin the lago;m closure by either removing the sludge remaining in the lagoon, for
disposal off-site, or by chemically fixing the sludge such\that disposal on-site can be
accomplished. All activities will be performed in strict accordance with applicable State, Federal,
2nd local environmental regulations.
If there are any remaining reasons why we cannot begin these activities, please advise us
immediately. We plan to initiate these steps a~ soon as ieather permits, h0pefully within the next
90 day~.
Thank you for your continuing assistance in this matter. I note that you have advised me that you
will no longer be project manager for this project. I assume that this notification will be
forwarded to your replacement.
Sincerely,
LEONHARDT ENVIRONMENT AL
I Ii~ -1 \I i'.1 v_._.__ --1~
. I: H. Derr Leonhardt II, PE I :· ..
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Consulting Services in
Ehgineering and the
I, Environment '
, · ,,,,.. .. I: .
CHEMICAL & ENVIRONMEN,TAL TECHNOLOGY, INC. I ENVIRONMENTAL ANAL YT/CAL SERVICES I
\ cc,N, eseo,s OS ,,,ccss(
I ½EONHARDT ENVIRONMENTAL
3,208 TWIN LEAF DR.
RALEIGH, NC 27613-
REPORT DATE, 02/24/98
1 A?tn, D. LEONHARDT , ..
.,. I CRISTEX LAGOON
SiMPLE NUMBER-141295
oiTE SAMPLED-01/30/98 I DATE RECEIVED-02/02/98
TIME RECEIVED-1037 , ..
I Page .,, 1 of 1
' I ANA1!YSIS
FLUORIDE
ARSENIC,TOTAL
I BARIUM, TOTAL
CADM~UM,TOTAL
CHROMIUM,TOTAL
I LEAD, TOTAL
MERCURY,TOTAL ,.
SELENIUM,TOTAL
SAMPLE ID-LAGOON WATER
SAMPLER-DERR LEONHARDT
DELIVERED BY-L. LEONHARDT
PROJECT NAME , CRISTEX LAGOON
METHOD
EPA340.2
206.2
200.7
200.7
200.7
239.2
245.1
270.2
\ SAMPLE PREP ANALYSIS
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DATE ly ::::2/98
02/04/98 □Pe 02/23/98
02/03/98 DPG 02/09/98 I 02/03/98 DPG 02/09/98 ' 02/03/98 DPG 02/09/98
I 02/04/98 DPG 02/06/98
' 02/05/98 DPG 02/06/98 I 02/04/98 DPG 02/24/98
SILVtR,TOTAL 200.7
I PQL l-Practical Quantitation Limit
' 02/03/98 DPG,02/09/98
estimated concentlations.
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Results followed by the letter J are
I NC DEHNR CERTIFICATIONS,
SAMPLE MATRIX-WW
TIME SAMPLED-1100
RECEIVED BY-LEB
BY RESULT UNITS
JTC < 0.1 mg/L
JMM <0.005 mg/L
JMM 0.013 mg/L
JMM <0.005 mg/L
JMM <0.005 mg/L
JMM 0.003 mg/L ~
DPG <0.0002 mg/L
JMM <0.002 mg/L
JMM <0.005 mg/L
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DWQ -96; PUBLIC WATER SUPPL\ -37724
LABORATORY DIRECTOR~~"'-!----~L-'-"~'J,aL)--V'~-"•CJUl'l-"ilP-<-4>~w,<'.,,(___)--""''----
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PQL
0.1
0.005
0.005
0.005
0.005
0.002
0.0002
0. 002
0.005
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I P.O. Box 12298 • Research Triangle Park. NC 27709
Telephone [phone]
I Shipping: 102-A Woodwinds Industrial Court • Cary, NC 27511
\, Fax\919\467-3515 r.
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CHEMICAL & ENVIRONMENTAL TECHNOLOGY, INC.
I
ENVIRONMENTAL ANAL YT/CAL SERVICES
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FINAL REPORT OF
LEONHARDT ENVIRONMENTAL
13'.,2., 0 8 TWIN LEAF DR.
RALEIGH, NC 27613-
Attn, D. LEONHARDT
ANALYSE\
REPORT DATE, 02/25/98
I C~ISTEX CORPORATION
SAMPLE NUMBER-141831 SAMPLE ID-SAMPLE #1
I DATE SAMPLED-02/13/98
DATE RECEIVED-02/13/98 SAMPLER-DERR LEONHARDT
TIME RECEIVED-1345 DELIVERED BY-L.L.D. I Page 1 of 3 PROJECT NAME , CRIS TEX COR•P.
I ANALYSIS
BAS:_~ NEUTRAL/ACIDS
ACENAPHTHENE
ACENAPHTHYLENE
AJ:!THRACENE I
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BENZIDINE
BENZO(a)ANTHRACENE
BENZO(b)FLUORANTHENE
BENZO(k)FLUORANTHENE
BENZO(g,h,i)PERYLENE
BENZO(a)PYRENE
bis;-(2-CHLOROETHYL) ETHER 'I bis:-(2-CHLOROETHOXY) METHANE
bis~(2-CHLOROISOPROPYL)ETHER
bi~t(2-ETHYLHEXYL) PHTHALATE
4-BROMOPHENYL PHENYL ETHER
sufiL BENZYL PHTHALATE
2 -C_HLORONAPHTHALENE
4-CHLOROPHENYL PHENYL ETHER
CHRYSENE
DIBENZO(a,h)ANTHRACENE
di-n'-BUTYLPHTHALATE
p'
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I SAMPLE PREP
METHOD DATE BY
\ EPA 625 02/18/98 AEK
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 62 5
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPI'. 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
ANALYSIS
DATE
02/24/98
I,
BY
SAMPLE MATRIX-WW
TIME SAMPLED-0800
RECEIVED BY-LEB
RESULT UNITS
JBR
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
11. 2 ug/L ~
< 10 ug/L
< 10 ug/L
< 10 ug/L
10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
PQL
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I P.O. Boxh' 2298 • Research Triangle Park, NC 27709
Telephorie [phone]
Shipping: 102-A Woodwinds Industrial Court • Cary, NC 27511
\, Fax[phone] ,, ,,
10
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10
10
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CHEMICAL & ENVIRONMENTAL TECHNOLOGY, INC.
ENVIRONMENTAL ANALYTICAL SERVICES
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Page 2 of 3 I CONTINUATION
PROJECT NAME , CRISTEX CORP.
OF DATA FOR SAMPLE NUMBER 141831
I ANALYSIS METHOD
SAMPLE PREP
DATE BY
1,2-DICHLOROBENZENE EPA 625
I 1,3-DICHLOROBENZENE EPA 625
1,4-DICHLOROBENZENE EPA 625
3,3'-DICHLOROBENZIDINE EPA 625
DIETHYL PHTHALATE EPA 625
I DIMETHYL PHTHALATE EPA 625
2,4-DINTROTOLUENE EPA 625
2,6-DINITROTOLUENE EPA 625
I di-n-OCTYLPHTHALATE EPA 625
FLUORANTHENE EPA 625
FLUORENE EPA 625
HEXACHLOROBENZENE EPA 625
I HEXACHLOROBUTADIENE EPA 625
HEXACHLOROCYCLOPENTADIENE EPA 625
HEXACHLOROETHANE EPA 625
INDENO(l,2,3-cd)PYRENE EPA 625
I ISOPHORONE EPA 625
NAPHTHALENE EPA 625
NITROBENZENE EPA 625
N-NITROSODIMETHYLAMINE EPA 625 I N-NITROSODIPHENYLAMINE EPA 625
N-NITROSODI-n-PROPYLAMINE EPA 625
PHENANTHRENE EPA 625
I PYRENE EPA 625
1,2,4-TRICHLOROBENZENE EPA 625
4-CHLORO-3-METHYLPHENOL EPA 625
2-CHLOROPHENOL EPA 625
I 2,4-DICHLOROPHENOL EPA 625
2,4-DIMETHYLPHENOL EPJ''.I. 625
2,4-DINITROPHENOL EPA 625
2-METHYL-4,6-DINITROPHENOL EPA 625
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ANALYSIS
DATE BY RESULT UNITS
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 20 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 20 ug/L
< 10 ug/L
PQL
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I P.O. Box 1 2298 • Research Triangle Park, NC 27709
Telephone [phone]
Shipping: 102-A Woodwinds Industrial Court • Cary, NC 27511
Fax[phone]
10
10
10
20
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
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10
20
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CHEMICAL & ENVIRONMENTAL TECHNOLOGY, INC.
ENVIRONMENTAL ANAL YT/CAL SERVICES
Page 3 of 3 I CONTINUATION
PROJECT NAME , CRISTEX CORP.
OF DATA FOR SAMPLE NUMBER 141831
I ANALYSIS
2-NITROPHENOL
4-NITROPHENOL
PENTACHLOROPHENOL
METHOD
EPA 625
EPA 625
EPA 625 I PHENOL EPA 625
2,4,6-TRICHLOROPHENOL EPA 625 I PQL = Practical Quantitation Limit
SAMPLE
DATE
PREP
BY
ANALYSIS
DATE
Results followed by the letter J are estimated concentrations. I NC DEHNR CERTIFICATIONS, DWQ -96; PUBLIC WATER SUPPLY -37724
BY RESULT UNITS
< 10 ug/L
< 20 ug/L
< 20 ug/L
< 10 ug/L
< 10 ug/L
I LABORATORY DIRECTOR ~ ~
PQL
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I P.O. Box 12298 • Research Triangle Park, NC 27709
Telephone [phone]
Shipping: 102-A Woodwinds Industrial Court • Cary, NC 27511
Fax {919) 467-3515
10
20
20
10
10
r
,Llab,Report D From: NC Certi£ication No. 402
SC Certi£ication No. 99012
D NC Drinking Water Cert. No.
FL Certi£ication No. E87519
37735 Full Service Analytical & Environmental Solul1011s
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April 6, 1998
To: Garco, Inc
Attn: Greg Russell
PO Box 1907
Asheboro, NC 27204-1907
Project: Cristex
The £allowing analytical results have been obtained £or the
indicated sample which was submitted to this laboratory:
Sample I.O. AA91138 Customer Code: GARCO
Login Group#: 2993D3 Customer Re£erence: CRISTEX
Phone Number: [phone]/£ax(336)683-0811
Customer Sample I.D#: INLET
Sample collection date: 03/16/98
Lab submittal date: 03/18/98
Received by: KSB
Parameter: TCLP EXTRACTION
Method re£erence: 1311
Result: Completed
Date started: 03/24/98
Time started: 19:00
Time: 14:30
Time: 10:00
Validated by:
Unit:
ADD
MDL or sensitivity:
Date £inished: 03/25/98
Analyst: DR2
Parameter: TCLP EXTRACTION <VOLATILES ONLY)
Method re£erence: 1311
Result: Completed
Date started: 03/19/98
Time started: 14:00
Parameter: METALS DIGESTION
Method re£erence: EPA 3010
Result: Completed
Date started: 03/25/98
Time started: 10:30
Parameter: PREP. METHOD 3510
Method re£erence: 3510
Result: Completed
Date started: 03/25/98
Time started: 15:00
Parameter: ARSENIC, LEACHABLE
Method re£erence: 6010
Result: Less than
Date started: 03/26/98
Time started: 10:00
Unit:
MDL or sensitivity:
Date £inished: 03/20/98
Analyst: DRR
Unit:
MDL or sensitivity:
Date £inished: 03/25/98
Analyst: DR2
Unit:
MDL or sensitivity:
Date £inished: 03/25/98
Analyst: DRR
Unit: mg/L
MDL or sensitivity: 0.50
Date £inished: 03/26/98
Analyst: LAM
449 Springbrook Road ,._ P.O. Box 240543 ,._ Charlorre, NC 28224-0543
Phone, 704/529-6364 ,._ Toll Free Number, 1-800/529-6364 ,._ Fax, 704/525-0409
, L.ab, Report 0 Garco, Inc
Page: 2
Sample I. D. AA91138 (continued)
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April 6, 1998
Parameter: SELENIUM, LEACHABLE
Method reference: 6010
Result: Less than
Date started: 03/26/98
Time started: 10:00
Parameter: CADMIUM, LEACHABLE
Method reference: 6010
Result: Less than
Date started: 03/26/98
Time started: 10:00
Parameter: CHROMIUM, LEACHABLE
Method reference: 6010
Result: Less than
Date started: 03/26/98
Time started: 10:00
Parameter: LEAD, LEACHABLE
Method reference: 6010
Result: Less than
Date started: 03/26/98
Time started: 10:00
Parameter: SILVER, LEACHABLE
Method reference: 6010
Result: Less than
Date started: 03/26/98
Time started: 10:00
Parameter: MERCURY, LEACHABLE
Method reference: 7471
Result: Less than
Date started: 03/26/98
Time started: 15:15
Parameter: BARIUM, LEACHABLE
Method reference: 6010
Result: Less than
Date started: 03/26/98
Time started: 10:00
Parameter: TCLP VOLATILES BY 8260
Method reference: SW846-8260
Result: see below
Date started: 04/01/98
Time started: 19:04
Full Service Analytical & Environmental Solutions
Unit: mg/L
MDL or sensitivity: 0.10
Date finished: 03/26/98
Analyst: LAM
Unit: mg/L
MDL or sensitivity: 0.10
Date finished: 03/26/98
Analyst: LAM
Unit: mg/L
MDL or sensitivity: 0.50
Date finished: 03/26/98
Analyst: LAM
Unit: mg/L
MDL or sensitivity: 0.50
Date finished: 03/26/98
Analyst: LAM
Unit: mg/L
MDL or sensitivity: 0.50
Date finished: 03/26/98
Analyst: LAM
Unit: mg/L
MDL or sensitivity: 0.02
Date finished: 03/26/98
Analyst: DR2
Unit: mg/L
MDL or sensitivity: 10.00
Date finished: 03/26/98
Analyst: LAM
Unit: mg/L
Date finished: 04/01/98
Analyst: MP
Parameter: TCLP SEMI-VOLATILES BY 8270
Method reference: 8270 Unit: mg/L
Result: see below
Date started: 04/01/98
Time started: 17:13
Date finished: 04/01/98
Analyst: MP
449 Springbrook Road • P.O. Box 240543 • Charlotte. NC 28224-0543
Phone, 704/529-6364. Toll Free Number, 1-800/529-6364. Fax, 704/525-0409
11 , Lab Report
IJ Garco, Inc
Page: 3
Sample I.D. AA91138 (continued)
April 5, 1998 Full Service Analytical & Environmental Solulions
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Parameter: MERCURY DIGESTION
Method reference: 7471
Result: Completed
Date started: 03/25/98
Time started: 11:00
Parameter: OIL & GREASE
Method reference: SM 5520E
Result: 170 mg/kg
Date started: 03/27/98
Time started: 09:00
Unit:
MDL or sensitivity:
Date finished: 03/25/98
Analyst: DR2
MDL or sensitivity: 10
Date finished: 03/27/98
Analyst: JAM
Parameter: CALCULATIONS BASED ON DRY WEIGHT
Method reference: SM 2540 G
Result: 55 ¼ DRY WT.
Date started: 03/24/98
Time started: 15:45
Data for TCLP VOLATILES
Component Kame
BENZENE
BY 8250 mg/L:
MDL or sensitivity: 0.01
Date finished: 03/24/98
Analyst: JAM
Result Component
Not detected 0.01
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~ CARBON TETRACHLORIDE
CHLOROBENZENE
Not detected 0.01
0.057 0.01
CHLOROFORM Not detected 0.01
1,4-DICHLOROBENZENE Not detected 0.014
1,2-DICHLOROETHANE Not detected 0.01
1,1-DICHLOROETHENE Not detected 0.01
METHYL ETHYL KETONE Not detected 0.04
TETRACHLOROETHENE Not detected 0.012
TRICHLOROETHENE Not detected 0.01
VINYL CHLORIDE Not detected 0.02
I Data for TCLP SEMI-VOLATILES BY 8270 mg/L:
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Component Kame Result Component
CRESOLS Not detected 0.050
1,4-DICHLOROBENZENE Not detected 0.050
2,4-DINITROTOLUENE Not detected 0.012
HEXACHLOROBENZENE Not detected 0.010
HEXACHLOROBUTADIENE Not detected 0.050
HEXACHLOROETHANE Not detected 0.050
NITRO BENZENE Not detected 0.050
PENTACHLOROPHENOL Not detected 0.25
PYRIDINE Not detected 0.25
2,4,5-TRICHLOROPHENOL Not detected 0.25
2,4,5-TRICHLOROPHENOL Not detected 0.10
Sample comments:
Project Name: Cristex
449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-0543
Phone, 704/529-6364 • Toll Free Number, 1-800/529-6364 • Fax, 704/525-0409
l'IDL
KDL
I\, Lab Report
If Garco, Inc
Page: 4
April 6, 1998
Sample I. D. AA91138 (continued)
2~~-
"l;'::\1.
'· c/'·
t(
Full Service Analytical & Environmental Solutions
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I£ there are any questions regar ata, please call.
Angela D. Overcash
Laboratory Director
449 Springbrook Road • P.O. Box 240543 • Charlene, NC 28224-0543
Phone, 704/529-6364 • Toll Free Number, 1-800/529-6364 • Fax, 704/525-0409
Full Service Analytical & Environmental Solutions
Client ___ (!AR.C._O~· ---~~~---------
Physical Addre~l--~c_, •~_F_,o_x_1_')_0_7~---------
PAGE_·_ OF __
449 Springbrook Road .... Charlotte, NC 2821 7
P.O. Box 240543 ..-. Charlotte, NC 28224-0543
Phone: [phone] ..-. Fax: [phone]
San:iples INT ~CT upon arriyal?
Re"ceived ON-WET rcE? Tem'P · · : -·• : • ,_ ~'.~. ! ·-.: _];_··•\--. --. -
PAOPER'PAESERVATJVES indicated?
'ReC~iVed "0riH1N HoL□iNG TIMES?
: cusrooY. sEALS IN.TACT?
:'"Vol..Ar1LEk ~Eic-·d'.W,Our·HEA□SPACE?
PAoPER· CoNTAINEAs ~-sed? · . . :". . -~, . . . '-.:. . ,
State Certification
As heboro, NC 27203
BILL TO:
Ad~ress-'\
Name ~ Requested NC --SC __ Other __ NA --
Phone 3_J 6 ·· 6 S 3 -ft'.LU __ Fax _13Ji=6Jl3=•l8_U_
P.0.#/Billing Reference ± Address ~---S--"-,--------~
Requested Due Date•~------'--.,~-------~
Water Chlorinated Yes No NA __
Sample Iced Upon Collection Yes __ No __
/1 •
Project Name _L..,.".:':1S -L.-~-----------~~ (SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
TIME MATRIX SAMPLE CONTAINER ANAL VSES REQUESTED SUB
;{/ Rt ~~4~r if// REMARKS
CLIENT DATE COLLECTED (SOIL, PRESERVA-LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR "TYPE . TIVES CERT.
HOURS SLUDGE) SEE BELOW NO. SIZE ~ ~t ;z0't~ < o/' o, ID NO.
.1,-, /4..~I--.
3/!t,,/_92_ SL~-.M)«,._ I~,,.-;; _y_ ,_er ,r y _/.£/3.Q__ -.?-.,-'_c_'7D~ ~W;U-~-
l}J •d_r, ' I J.!/3-r ,2 h . x:: y / ,( _ '-.OJJ:L-f= I I I( /{ I ( I: . I I{ iSD.D t( ? L _L_ _J~ L _D.,, __ /,.-r {( ,, '
.
.
,J / r> v
Sampler's Signature _4-,:..f/hn£..0 Sampled By (Pr;nt Name) -&--v:,-~f C // Affiliation
,.--. -. :.-I ' R:?t:~-~y~-~:~):R' Received By: (Signature) V Date Military/Hours Addition.al Comments:
-_%_£ ~ -.
Relinquished By: (Signature) ' · Received By: (Signature) Date
Relinquished By: (Signature) Received For Prism laboratories By: Date
_____i(_~.uy-,.&d1, ¾eL"liL _;a..a.u _
MethodCli.Shipment: log-In Group No.
);//'/ -:-:, '") 7
NPDES: NC ---·usT: NC __ _ GROUNDWATER: NC __ _ DRINKING WATER: NC __ _ SOLID WASTE: NC ___ . OTHER: NC~--
SC __ _ SC __ _ SC __ _ SC __ _ SC __ _ SC __ _
OTHER OTHER OTHER __ OTHER OTHER __ OTHER
*CONTAINER TYPE CODES: A == Amber C = Clear G == Glass P = Plastic; TL= Teflon-Lined Cap. VOA= Volatile Organics Analysis (Zero Head Space)
'SEE REVERSE FOR· -, '
TEAMS & CONDITIONS-._
PRISM
LAB
IONO.
~
. D1;,IJ ·-'-'-
t_J}..!_/'i
FINAL REPORT COPY
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Lab Report
From: NC Certification No. 402
~&, . >·
mmlliiiiise&'.~~-( SC Certification No. 99012
NC Drinking Water Cert. No.
FL Certification No. E87519
37735 Full Service Analy11cal & Environmental Solutions
April 6, 1998
To: Garco, Inc
Attn: Greg Russell
PO Box 1907
Asheboro, NC 27204-1907
Project: Cristex
The following analytical results have been obtained for the
indicated sample which was submitted to this laboratory:
Sample I.D. AA91139 Customer Code: GARCO
Login Group#: 2993D3 Customer Reference: CRISTEX
Phone Number: [phone]/fax[phone]
Customer Sample I.D#: MIDPOINT
Sample collection date: 03/16/98 Time: 14:45
Lab submittal date: 03/18/98 Time: 10:00
Received by: KSB
Parameter: TCLP EXTRACTION
Method reference: 1311
Result: Completed
Date started: 03/24/98
Time started: 19:00
Validated by: ADO
Unit:
MDL or sensitivity:
Date finished: 03/25/98
Analyst: DR2
Parameter: TCLP EXTRACTION (VOLATILES ONLY>
Method reference: 1311
Result: Completed
Date started: 03/19/98
Time started: 14:00
Parameter: METALS DIGESTION
Method reference: EPA 3010
Result: Completed
Date started: 03/25/98
Time started: 10:30
Parameter: PREP. METHOD 3510
Method reference: 3510
Result: Completed
Date started: 03/25/98
Time started: 15:00
Parameter: ARSENIC, LEACHABLE
Method reference: 6010
Result: Less than
Date started: 03/26/98
Time started: 10:00
Unit:
MDL or sensitivity:
Date finished: 03/20/98
Analyst: DRR
Unit:
MDL or sensitivity:
Date finished: 03/25/98
Analyst: DR2
Unit:
MDL or sensitivity:
Date finished: 03/25/98
Analyst: DRR
Unit: mg/L
MDL or sensitivity: 0.50
Date finished: 03/26/98
Analyst: LAM
449 Springbrook Road • P.O. Box 240543 • Char[o[le, NC 28224-0543
Phone, 704/529-6364 • Toll Free Number, 1-800/529-6364 • Fax, 704/525-0409
1·
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Lab. Report
Garco, Inc
Page: 2
Sample I.D. AA91139 (continued)
April 5, 1998
Parameter: SELENIUM, LEACHABLE
Method reference: 5010
Result: Less than
Date started: 03/25/98
Time started: 10:00
Parameter: CADMIUM, LEACHABLE
Method reference: 5010
Result: Less than
Date started: 03/25/98
Time started: 10:00
Parameter: CHROMIUM, LEACHABLE
Method reference: 5010
Result: Less than
Date started: 03/25/98
Time started: 10:00
Parameter: LEAD, LEACHABLE
Method reference: 5010
Result: Less than
Date, started: 03/25/98
Time. started: 10:00
Parameter: SILVER, LEACHABLE
Method reference: 5010
Result: Less than
Date started: 03/25/98
Time started: 10:00
Parameter: MERCURY, LEACHABLE
Method reference: 7471
Result: Less than
Date started: 03/25/98
Time started: 15:15
Parameter: BARIUM, LEACHABLE
Method reference: 5010
Result: Less than
Date started: 03/25/98
Time started: 10:00
Parameter: TCLP VOLATILES BY 8250
Method reference: SW845-8250
Result: see below
Date started: 04/01/98
Time started: 19:45
Full Service Analytical & Environmental Solu11ons
Unit: mg/L
MDL or sensitivity: 0.10
Date finished: 03/25/98
Analyst: LAM
Unit: mg/L
MDL or sensitivity: 0.10
Date finished: 03/25/98
Analyst: LAM
Unit: mg/L
MDL or sensitivity: 0.50
Date finished: 03/25/98
Analyst: LAM
Unit: mg/L
MDL or sensitivity: 0.50
Date finished: 03/25/98
Analyst: LAM
Unit: mg/L
MDL or sensitivity: 0.50
Date finished: 03/25/98
Analyst: LAM
Unit: mg/L
MDL or sensitivity: 0.02
Date finished: 03/25/98
Analyst: DR2
Unit: mg/L
MDL or sensitivity: 10.00
Date finished: 03/25/98
Analyst: LAM
Unit: mg/L
Date finished: 04/01/98
Analyst: MP
Parameter: TCLP SEMI-VOLATILES BY 8270
Method reference: 8270
Result: see below
Date started: 04/01/98
Time started: 17:54
Unit: mg/L
Date finished: 04/01/98
Analyst: MP
449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-0543
Phone, 704/529-6364. Toll Free Number, 1-800/529-6364. Fax, 704/525-0409
. Lab Report I Garco, Inc
Page: 3
Sample I.D. AA91139 (continued)
•:
:i(·
' y
.~~ ,,~~;
I April 6, 1998 Full Service Analytical & Env1ronmental Solulions
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Parameter: MERCURY DIGESTION
Method reference: 7471
Result: Completed
Date started: 03/26/98
Time started: 11:00
Parameter: OIL & GREASE
Method reference: SM 5520E
Result: 2500 mg/kg
Date started: 03/27/98
Time started: 09:00
Unit:
MDL or sensitivity:
Date finished: 03/26/98
Analyst: DR2
MDL or sensitivity: 10
Date finished: 03/27/98
Analyst: JAM
Parameter: CALCULATIONS BASED ON DRY WEIGHT
Method reference: SM 2540 G
Result: 52 1/. DRY WT.
Date started: 03/24/98
Time started: 15:45
Data for TCLP VOLATILES BY 8260 mg/L:
MDL or sensitivity: 0.01
Date finished: 03/24/98
Analyst: JAM
I Component Name
BENZENE
Resul.t
Not detected
Component
0.01
Not detected 0.01 _ , CARBON TETRACHLORIDE
':::::.)CHLOROBENZENE I ,CHLOROFORM
~1,4-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,1-DICHLOROETHENE
METHYL ETHYL KETONE
0.330 0.01
Not detected 0.01
0.027 0.014
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TETRACHLOROETHENE
TRICHLOROETHENE
VINYL CHLORIDE
Not
Not
Not
Not
Not
Not
detected
detected
detected
detected
detected
detected
Data for TCLP SEMI-VOLATILES BY 8270 mg/L:
Component Name Resul.t
CRESOLS Not detected
1,4-DICHLOROBENZENE Not detected
2,4-DINITROTOLUENE Not detected
HEXACHLOROBENZENE Not detected
HEXACHLOROBUTADIENE Not detected
HEXACHLOROETHANE Not detected
NITROBENZENE Not detected
PENTACHLOROPHENOL Not detected
PYRIDINE Not detected
2,4,5-TRICHLOROPHENOL Not detected
2,4,6-TRICHLOROPHENOL Not detected
Sample comments:
Project Name: Criste><
0.01
0. 01
0.04
0.012
0.01
0.02
Component
0.050
0.050
0.012
0.010
0.050
0.050
0.050
0.25
0.25
0.25
0.10
449 Springbrook Road ...., P.O. Box 240543 ..,. Charlotte, NC 28224-0543
Phone: [phone] .... Toll Free Number: l -800/529-6364 .... Fax: [phone]
HDL
HDL
I , Lab Report
Garco, Inc
Page: 4
Sample I. D. AA91139 (continued)
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April 5, 1998 Full Service Analytical & Environmental Solutions
I£ there are any questions reg~rding a, please call.
Angela D. Overcash
Laboratory Director
449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-0543
Phone, 704/529-6364 • Toll Free Number, t-800/529-6364. Fax, 704/525-0409
. Lab Report I From: NC Certification No. 402
SC Certification No. 99012
I NC Drinking Water Cert. No.
FL Certification No. E87519
37735 Full Service Analytical & Environmental Solutions
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April 6, 1998
To: Garco, Inc
Attn: Greg Russell
PO Box 1907
Asheboro, NC 27204-1907
Project: Cristex
The following analytical results have been obtained for the
indicated sample which was submitted to this laboratory:
Sample I.D. AA91140 Customer Code: GARCO
Login Group#: 2993D3 Customer Reference: CRISTEX
Phone Number: [phone]/fax[phone]ll
Customer Sample I.D#: OUTLET
Sample collection date: 03/16/98 Time: 15:00
Lab submittal date: 03/18/98
Received by: KSB
Parameter: TCLP EXTRACTION
Method reference: 1311
Result: Completed
Date started: 03/24/98
Time started: 19:00
Time: 10:00
Validated by: ADO
Unit:
MDL or sensitivity:
Date finished: 03/25/98
Analyst: DR2
Parameter: TCLP EXTRACTION (VOLATILES ONLY)
Method reference: 1311
Result: Completed
Date started: 03/19/98
Time started: 14:00
Parameter: METALS DIGESTION
Method reference: EPA 3010
Result: Completed
Date started: 03/25/98
Time started: 10:30
Parameter: PREP. METHOD 3510
Method reference: 3510
Result: Completed
Date started: 03/25/98
Time started: 15:00
Parameter: ARSENIC, LEACHABLE
Method reference: 6010
Result: Less than
Date started: 03/26/98
Time started: 10:00
Unit:
MDL or sensitivity:
Date finished: 03/20/98
Analyst: DRR
Unit:
MDL or sensitivity:
Date finished: 03/25/98
Analyst: DR2
Unit:
MDL or sensitivity:
Date finished: 03/25/98
Analyst: ORR
Unit: mg/L
MDL or sensitivity: 0.50
Date finished: 03/26/98
Analyst: LAM
449 Springbrook Road. P.O. Box 240543 • Charlorre, NC 28224-0543
Phone, 704/529-6364 • Toll Free Number, 1-800/529-6364. Fax, 704/525-0409
I' la~a~~:~:~ Sample I.D. AA91140 (continued)
".-:::t.~ ~r
c~:
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Page: 2
April 6, 1998
Parameter: SELENIUM, LEACHABLE
Method re£erence: 6010
Result: Less than
Date started: 03/26/98
Time started: 10:00
Parameter: CADMIUM, LEACHABLE
Method re£erence: 6010
Result: Less than
Date started: 03/26/98
Time started: 10:00
Parameter: CHROMIUM, LEACHABLE
Method re£erence: 6010
Result: Less than
Date started: 03/26/98
Time started: 10:00
Parameter: LEAD, LEACHABLE
Method re£erence: 6010
Result: Less than
Date started: 03/26/98
Time started: 10:00
Parameter: SILVER, LEACHABLE
Method re£erence: 6010
Result: Less than
Date started: 03/26/98
Time started: 10:00
Parameter: MERCURY, LEACHABLE
Method re£erence: 7471
Result: Less than
Date started: 03/26/98
Time started: 15:15
Parameter: BARIUM, LEACHABLE
Method re£erence: 6010
Result: Less than
Date started: 03/26/98
Time started: 10:00
Parameter: TCLP VOLATILES BY 8260
Method re£erence: SW846-8260
Result: see below
Date started: 04/01/98
Time started: 20:26
Parameter: TCLP SEMI-VOLATILES BY 8270
Method reference: 8270
Result: see below
Date started: 04/01/98
Time started: 18:40
Full Service Analytical & Environmental Solutions
Unit: mg/L
MDL or sensitivity: 0.10
Date £inished: 03/26/98
Analyst: LAM
Unit: mg/L
MDL or sensitivity: 0.10
Date £inished: 03/26/98
Analyst: LAM
Unit: mg/L
MDL or sensitivity: 0.50
Date £inished: 03/26/98
Analyst: LAM
Unit: mg/L
MDL or sensitivity: 0.50
Date £inished: 03/26/98
Analyst: LAM
Unit: mg/L
MDL or sensitivity: 0.50
Date finished: 03/26/98
Analyst: LAM
Unit: mg/L
MDL or sensitivity: 0.02
Date finished: 03/26/98
Analyst: DR2
Unit: mg/L
MDL or sensitivity: 10.00
Date finished: 03/26/98
Analyst: LAM
Unit: mg/L
Date finished: 04/01/98
Analyst: MP
Unit: mg/L
Date finished: 04/01/98
Analyst: MP
449 Springbrook Road • P.O. Box 240543 • Charlotte. NC 28224-0543
Phone, 704/529-6364 • Toll Free Number, 1-800/529-6364 • Fax, 704/525-0409
I . Lab Report
Garco, Inc
Page: 3.
Sample I.D. AA91140 (continued)
I April 6, 1998 Full Service Analytical & Environmental Solutions
I
I
Parameter: MERCURY DIGESTION
Method re£erence: 7471
Result: Completed
Date started: 03/26/98
Time started: 11:00
Parameter: OIL & GREASE
I \Method re£erence: SM 5520E
~Result: 8600 mg/kg
Date started: 03/27/98
Time started: 09:00
Unit:
MDL or sensitivity:
Date £inished: 03/26/98
Analyst: DR2
MDL or sensitivity: 10
Date £inished: 03/27/98
Analyst: JAM
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Parameter: CALCULATIONS BASED ON DRY WEIGHT
Method re£erence: SM 2540 G
Result: 69 Y. DRY WT.
Date started: 03/24/98
Time started: 15:45
Data £or TCLP VOLATILES BY 8260 mg/L:
I Component Harne
----0BENZENE
~CARBON TETRACHLORIDE
I -==-'-CHLOROBENZENE > CHLOROFORM
-1,4-DICHLOROBENZENE
1,2-DICHLOROETHANE I 1,1-DICHLOROETHENE
METHYL ETHYL KETONE
TETRACHLOROETHENE
TRICHLOROETHENE
VINYL CHLORIDE
MDL or sensitivity: 0.01
Date £inished: 03/24/98
Analyst: JAM
Result Component
0.073 0.01
Not detected 0.01
0.730 0.01
Not detected 0.01
0.020 0.014
Not detected 0.01
Not detected 0.01
Not detected 0.04
Not detected 0.012
Not detected 0.01
Not detected 0.02 I
I Data £or TCLP SEMI-VOLATILES BY 8270 mg/L:
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Component Harne Result Component
CRESOLS Not detected 0.050
1,4-DICHLOROBENZENE Not detected 0.050
2,4-DINITROTOLUENE Not detected 0.012
HEXACHLOROBENZENE Not detected 0.010
HEXACHLOROBUTADIENE Not detected 0.050
HEXACHLOROETHANE Not detected 0.050
NITROBENZENE Not detected 0.050
PENTACHLOROPHENOL Not detected 0.25
PYRIDINE Not detected 0.25
2,4,5-TRICHLOROPHENOL Not detected 0.25
2,4,6-TRICHLOROPHENOL Not detected 0.10
Sample comments:
Project Name: Cristex
449 Springbrook Road ~ P.O. Box 240543 ~ Charlotte, NC 28224-0543
Phone, 704/529-6364 ~ Toll Free Number, l-800/529-6364 ~ Fax, 704/525-0409
MDL
MDL
I , Lab Report
Garco, Inc
Page: 4
Sample I. D. AA91140 (continued)
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April 5, 1998 Full Service Analytical & Environmental Solutions
If there are any questions regarding this data, please call.
A
Laboratory
449 Springbrook Road A P.O. Box 240543 A Charlortc. NC 28224-0543
Phone, 704/529-6364 A Toll Free Number, t-800/529-6364 A Fax, 704/525-0409
i ·.. JIPII ol!llt~S J b
-;·_;:;,:{,;t';'.'..:·~:~,;·,:~;• ,·.-· ··: · · PAGE __ OF_._ .
j:::J,',]':{fi:i,449iSp~ingbrook Road ...,. Charlotte, NC 2821 7
:Jj''.i':,')tp'.ofBoX240543:... Charlotte, NC 28224-0543 i:t f., S~i~i;,'}04/529-.?~.?4. ""';. Fax: [phone]
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Full Service'Analytical &· Enitironmental:Solutions ,, ! ''"°""·.
Saf!'lplei_J lt-;l_T~CT tipon arrival? .
Received ON WET IC~? Temp -~-
PROPER PRESERVATIVES indicated? .,, '
Received WITHIN HOLDING TIMES?
~CUSTODY: SEALS INTACT?
vOLATILE.S r.ec'd.W/OUT HEADSPACE?
-PROPER·CONTA.INERS\ised.?. -;;,us.~;. ~~:::c::'i~~~~,i~~~:i~~,:;1,~g? ;J~-f j :· ..
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. BILL TO:.· Name---~-.-..,~----------
State Certification
Requested NC __ SC __ Other __ NA --
Water Chlorinated Yes No NA Phone[phone] . Fex 336 683-0811 Add,ess ::::-..., I ~--~ ... ...____-. ------Sample Iced Upon Collection Yes __ No __
P._0:#1a111~ng ~:~!_er,rce -:.z""· ~------'-_Ji'-,_.-.-.----'---~ Req':,lested Due Date
;Project Name _L.r~r, (SEE REVERSE SIDE FOR.RUSH TURNAROUND FEES)
'•.-. . ·: .. \:• ·'" ;'1'{ ·:.:{.TIME MATRIX. SAMPLE CONTAINER: //4~½;;;/4;~;~;/ / SUB
CLIENT . ' DATE COLLECTED (SOIL; PRESERVA~ LAB
SAMPLE DESCRIPTION COLLEC!ED · . MILITARY WATEROR "TYPE TIVES REMARKS CERT.
HoyRs I SLUDGE) SEE BELOW NO. SIZE IONO.
I;./4_/-.3/14/~ , . I SL~ _Mfak_ _.z._ l~d. . ' _,t r y ,Y _J_i/1,_!2_ .-i.Alo.N.L
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NPDES: NC ___ UST: .. NC ---s-
SC ___ SC __ ,_
OTHER__ OTHER __ :_
GROUNDWATER: NC __ _
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OTHER __
SOLID WASTE: NC __ _
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OTHER: NC __ _
SC __ _
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*CONTAINER TYPE CODES: A = Amber C := Clear G = Glass P = Plastic; TL= Teflon-Lined Cap VOA= Volatile Organics Analysis (Zero Head Space)
' SEE REVERSE Fon~ ...
.:.TERMS & CONDITIONS,""
PRISM
LAB
ID NO.
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91elL
1.fl!iJ_
ORIGINAL
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DATE:
TO:
FROM:
SITE:
March 11, 1999
File
Jeanette Stanley
Environmental Chemist
NC Superfund Section
Cristex Drum Site
NCO 001606250
Oxford, Granville County, North Carolina
I spoke with Mr. H. Derr Leonhardt II, PE, consultant for the Cristex site [phone]
regarding the data he provided to the NC Superfund Section on the lagoon sampling. The data
package did not contain volatile analyses of the lagoon water, only metals, fluoride, and
semi volatiles. I asked if I was missing the data or if the water sample was analyzed for volatiles.
He said that he had talked with a state employee in the Water Quality Section and had been advised
that since the water had been sitting in the lagoon for years, it was probably just rainwater and
analysis for volatile components was not necessary. He had not analyzed the impoundment water
for volatiles.
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To:
From:
Subject:
Date:
MEMORANDUM
File
~J Domia Wilson vp
Environmental Engineer
North Carolina Superfund Section
Magnetometer survey
Cristex Drum Site
Oxford, Granville County
June 11, 1998
Ref 16
On June 1, 1998, Dave Mattison and I conducted a mag1,etometer , urvey at the
above referenced site. We arrived at the facility at approximately 9:30 and met with Derr
Leonhardt of Leonhardt Environmental, consultant for George Christiansen. Mr.
Leonhardt stated that the sidewall in the lagoon next to the sewer inlet had been cut out to
allow the lagoon to drain. Samples were taken of the surface water and the sludge before
the surface water was discharged. He said that the Water Quality Division reviewed the
analysis and did not object to the discharge of the water to the tributary to Fishing Creek.
He gave me a copy of the analysis.
We walked to the former drum site, the barren area, :1nd the lagoon. The lagoon
still contains water throughout the bottom, apparently caused by a low permeable layer
and/or slope of the bottom of the lagoon away from the sidewali opening. The area is
overgrown with briars, brush, and blackberries, which made it very difficult to locate the
berm.
Beginning at t!:e south end of the berm, we began marking locations with wooden
stakes for magnetometer readings. We first placed stakes on the crest of the berm, every
five feet, in a straight line, N 20° W, from the south end of the berm to the north encl, with
the use of a I 00 foot tape measure (row c). We placed 20 stakes, which extended 95 feet.
Although I had initially estimated the berm length to be approximately 30 feet during the
March 1998 reconnaissance, on this day it was not possible to determine the distinct
boundaries of the berm due to the thick vegetation, approximately 3 to 5 feet high. The
north, south, and cast edges of the berm were gradually sloped, but the western edge was
more sloped. Each station was numbered from 1 to 20, south to north. We then returned
to the south end of the berm and placed stakes perpendicular to the original line, at each
station, on 5 foot centers, from station 2 to station 8, with the use of a compass (rows b
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Memorandum
Cristex Drum Site
Page 2
and d). Adjacent points for station I were not marked because it did not appear to be part
of the berm. We stopped at station 8 because there were not enough wooden stakes to
continue.
Magnetometer readings were obtained for the 22 marked points. Dave Mattison
operated the magnetometer and I recorded the readings. The magnetometer is
manufactured by Geometrics and its model number is G816/826A, Serial No. 6527. The
magnetometer is worn in straps over the shoulders and the magnet is placed vertical on
top of a 4 foot rod. Three readings were taken at each point, so that an average could be
obtained. After taking the first 3 readings, it was discovered that the box we had carried
to the berm containing some metal objects (hammer, compass, etc.) was close to statior2 1.
The box was moved approximately 20 feet away. After completing the readings for
stations I -8, we returned to stations I and 2 and took new readings, to correct for any
influence of the objects in the box.
Al approximately 11 :30, while we were obtaining the readings described above,
Derr Leonhardt left the site.
Dave Mattison and I removed some of the stakes from stations I -8 to reuse for
additional stations. We then measured and placed wooden stakes for stations 9 -14,
again using the compass to place the stakes perpendicular lo the center line c. We were
not able to place stakes on row d at stations 13 and 14 because the briars and brush were
too thick. A new western row, a, was added for those stations, which were on the side
slope of the berm.
We broke for iunch at 12: I 5 and returned to the site at I: 15.
Readings were taken for stations 9 and IO and we observed that the numbers were
lower on the eastern side of the berm (row b) in comparison to the readings for the other
rows. Readings on row b were measured with the magnet to the left (west) of the
instrument for convenience in dealing with the briars on stations 5 -9, while the readings
on rows c and dwere measured with the magnet to the right (east) of the instrument. We
tested one point on station IO by taking measurements with the magnet in both positions
and discovered a gamma difference of 40. All subsequent measurements were consistent
with positioning and row b readings from stations 5 -9, which were influenced by the
thick briars, were remeasured. Measurements taken on stations I -4 were not affected.
After completing the readings for row b on stations 5 -9 and the readings for
stations 9-14, some of the stakes were removed and reused on stations 15 -20. On
stations 15, 18, I 9, and 20, row d was deleted and row a was added because of the
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Memorandum
Cristex Drum Site
Page 3
shape of the berm.
After completing all magnetometer readings, Dave Mattison scanned the metal
detector in a sweeping motion over the study area. One precise "hit" was found between
stations 19 and 20 on the slope of the berm. We could find no visible source at the
ground surface. The spot was marked with a wooden stake. No other anomalies were
noted on the berm. We also scanned the barren area with the metal detector and found no
anomalies.
After driving by the Oak Ridge apartment complex and Maple Street, the
residential street closest to the surface water point of probable entry, we left Oxford at
approximately 3:45.
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Ref 17
CITY OF OXFORD. NORTH CAROLINA 27565
120 WILLIAMSBOF<O ST"EET. PO BOX 506 -<9191 693·2195
OFFICEOFT~◄E
CITY MANAGEl'-1
Mr. Robert P. Clewell
Pl ant Manager
Cristex Corporation
Indus try Ori ve
Oxford, N. C. 27565
Dear Mr. Clewell:
January 26, 1981
Re: Proposed Increase in
City Water and Waste
Treatment Capacity
Pursuant to your request this is to advise you that the proposed
increase in Cristex Corporation's use of water and waste treatment facil-
ities in the range of about 15% above current usage presents no problem to
the Oxford Water Works. It is approved.
We welcome this change because we are now in a position to furnish
adequate water and waste treatment to industrial customers.
On behalf of the Mayor and Board of Commissioners, the public at large
and myself we are happy to hear about your expansion and extend you our
best wishes for your continued success as a member of the Oxford industrial
COITITIUn i ty.
HTR, Jr /ap
cc: Mayor Hugh M. Currin
City Engr. Jesse Sullins
Jimmy Crews, Public Works Director
Oscar Dean, W & S Mntce. Superintendent
William Newton, Chief W.P. Operator
William Pritchett, Chief W.T.P. Operator
CD
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. -DIVISION OF ENVIRONMENTAL /.1.ANAGEMENT
June 26, iaai
l1EUORANDUM
TO.·
SUBJECI':
. u-til·[a,;,1 C. ·:~1-i?-7:.s.J Sup0rv-;.:Doi.,,.,
NPDES Permit• Um'.t
}~enneth ,)'c;'-1ut!te1·• .,td..,1..,,
Acting Regional, Supervisor
Raleigh J1es·{onal Office
CT·is-te:.c Co1·,noratio;i ' ' ' Revenue Bond_ Cert,[ficction ·
GranviUc Countu
, ___ LLirit,(_
--.. c:
'-)L(,;:C1/(.,L.
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Hefel.101Ce-·i::.: rt:a.:.-:3 ·f;o -:;:·:,.:; thcie .~.3., lJBZ.·IcrC"te2'l j':l•om :~.ir. Bill CouZte.'!1,
F"lant bngi;·iee:..1 ~ C:.•iu (;.3.;; Cc,:';_.:C!.•,::;:;-~o.~i coiiocrni:-iJ ·t:r3{1~ ;? J.,C!n,;ic,) c~.:r,,c:1-:.s-ion rirocro:m.
Tha Zet'Cer ··l;-~2:iccd;J;; i,i::..?.t tJ·2e present z . ..:::::0t0:Xit,.;;_~ f'Zot:· fi1oiii the Cy-iistex
•,.,in•n.~·-,,,._.· r. P'2" -=·~,.)· ..• 7-0•-1.·, ··1-,-,, •, __ .,., .. :.:., --,./ .i."'t,,,,-~ -i·-1: ·• ••.. , ·'-.--,,,,,,.-·f:r,•') ·,i,;,·,.,ov 01.,,· ,. .. ,..,+ • .,m • ,,,,..,.., v v~ i).J vuv;; Jc,,,_ -'JI:~:,/,, :_~v L-t:.-..'. , .. ...,,~1,;1. (..,.,._ v,_.._•,v ·'"J (,. ,,,,,. ,_.,.,.,A,,,,-o..:. "· ,_._.,. ,.::, .~/ c.:,'.:;._,,:.,.'
i.s ·instr..Z it>.1 t,;d,,;; fl.0.:--1 :.:,~ouZ:Z "i:,,.,; .t'e(f{ced 4 3. ;)~~-~-~·c;;,_:eueY3 t,'i,;,; ::--.~1.:x::oaed i1?arease
in j'Zow .reauZt·ltsr-r~.,r:.: . .-; -;;;·;c ·Z-1·!.::to.IZcJ.t·loi·~ o_; c:. (te:.:.1 7_,,ci~:5::.·· ,._-:usce1_·.c.t-c~,f ~-;it/, t}re ex-
pc::ts-lc-;-i p:i'O;J•i."'>C:J;1 i..:. rte.!;; c:2.:-.::..,:..:'.:JSc::-_:{.
Ffcce;;":; r1-;or;-~ :;:-,'!_'i1:;J· -:.\:t.(~ r,Jcciv.;;:5 for t/1..G· :210;_:;,;~ c/ 0."T;for•.'.~-, f! Southsi.( .. ~e
f.':.!ste~:c:.te1., ?1.•.::ri:tr..-:,J,Ti; ~::la-·!·; 1~:-!I!ccr-~ea t:·zat ·it ·ia. r:of-. :.:L'ov{J·i,;·-;,0· ::-1 . .:"lequate tr'lco:i;-
rr.s;it. 11/u;r.;fcric.. in c.c:.:01".J.::nce 1.,_;i-th iJCGS Zt.16'--.8 Z5 .. J?.:, tie. could n6t recomrrend
·that· t~e CePt-ifl;at·ioil i>a JJ.'1(1.n.ted if thzre ·will ~'e co-: increase i;~ wastewater'
flow to the 2.101-vn of C;.;:j'o~"):1 's sb· stem.. ·
1'hus, if a Certification is granted it should contain a stipulation
that the· wastewater l'ecovery system be installed as pa.rt of the expansion pro-
gram and tlzat there be no net· increase in wasteuJater· as .a rem, U · of the project.
. '~ RaZ..ngh ~sgionaZ Office haa no chJsct-lon to thia Cnotif-lcat-lon with ths above msnti.oned ati.puZ.at-lon. . ·. . . ·y.' ··. . ···.: · · · · . l!S/Jf-lR/tbj , . . ·. . . .
I·. ' .,;;,,/'•:;,
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RALEIGH REGI,ONAL OFFICF..
February 11, 1982
MEMORANDUM
TO: .FILE
BY: R.H. Ferneyhough
SUBJECT: Complairu:.,_ Heated-vate~. ischi,.rge
r-~ristex Coi:p. .·
. '--._ Oxford, Granville Count~.--.---
On February 3, 1982 the.RRO.office received
City of Oxford, concerning subject discharge.
a call. from Mr. -W. Pritchett,
Investigation on February 8 revealed a discharge of heated ,water in a ditch
running around the lagoon;
Mr. W. S. Brice, plant manager, and Mr. W. J. ·Coulter, plant engineer were.
contact.ed. • A tour of pla.nt grounds revealed that the waste line from the plant ··
to the lagoon had broken, thereby allowing the waste to enter the ditch. It was
requested that the line be repaired immediately and this office notified.
I
· Mr. Coulter called on· February 11 and stated that they had put a berm of ·
planks mid earth to divert the flow into the lagoon. They are in the process of
. getting a contractor to put in a new discharge line'.
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CIT.Y. 0JS OXf:ORD
□ FILE._ NO Re!PONSE D FILE. W!COPY REPLY.
,.·•:.--,
,.lt.••::,,::;t1 !3ul.] i11•=;
Ci ts En:Jinet::ir
F, 0, E<u:, :,06
A•.isust 12, l?8:l
120 Willie11,si1(Jre Stree·L
a~:fo1·ri, N.C. 27565
REC'D HJG I 8 1983
D COPY(IES) TO
D REROUTETO
D RESPONSE ON TAPE
Section 403,12 (bl of the Federal Pretreatment Regulations
140 CFR rart 403) and section ,0908 (bl of the State Pretreal-
ment Resulations 115 NCAC 2H ,0900) state that within 180 d2us
after the promulsation of a Pretreatment standard Industrial
lJsers subJect. to the star,daid shall be reauired to subn1it a 1·e-·
Port or·1 the nature arid cor,cer·1tratior1 of their dischar~e Ca bai~2·-
l.ir,e monitorin9 rePort). Enclosed sou will find a Package cun·-
t a i 1·, i r, g ':;>ever a 1 items th 1~ f i rs t being a l is t of categoric a 1 st:; 11 d ---
a 1· d s which have beer, pron,ulgated ir, final forn,. The list ir1cljJ(i(:
the date and Pa!;le of the Federal Resister in which• the resulati,i,,
af,pears as well as the effective date of the resulatio~. Wilhir1
lBO dass of the listed effective date ans Industrial Lise,, ( IU) ,,,..ii,··
Je ct Lo the ca teso 1-i cal standard n,us t subn, i l to the POTW a bas,, 1:i. ,,,,
ffiQr1itc,rir1S report. A coP~ of this repo1·t should be forward2d l\>
Lhe State's Pretreatment Offices,
The baseline ffionitorins rePort IBMR) submitted bs the Ill si1uul,J
cuntain all of the. information reouired bs 40 CFR Pa,t 403,l~ll•l
(1-7) and bs 15 NCAC 2H ,0908 (bl 11-7), Included in the enclosed
Packise is a surumijr~ 6f the.BMR reauirements arid a s-~in,F·le BMR
Fur m • This form is included as or, e }: am P 1 e and i. t is r1 fJ t :11 ~' r, ,. \ i --
tors for the IU to sPecificalls use this exact form, H0~E~er, I.he
i1·1forn1alior1 reauested on tt1is fo1·ru is sufficier1t to C8n1Pl~ wj_t~~
both 40 CFR Part 403,B lb) 11-7) and 15 MC.C,C 2H ,0908 '.i,) -:t-n,
Some of the Ills subJect to the finalized cat2icrical standa1·ds
ccl1)tained ir1 the enclosed Packa~e tt1a~ have ~l1·ead~ subn1itted a base-
line rePurt to EPA or to the State, If this ,s Lhe case the P □TW
sho1Jld re8uest a_ coP~ of the 1•eport arid check. il for con1Pliar1ce wi·tl,
40-CFR Part 403,12 lb) and 15 NCAC 2H ,0908 (bl,
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r f·11.:::, t, 2:: t i l t.:.• j_ 1 ·1 i:.) 1~1 s t r •,:: ·' '.:i-f: MF: r· en u i rt? 111 e n t s
frc1m tl·1e i:·1d•JStrial 1Js0r reuu:i~en1e1·~ts listed ir1 iten1
S1..11hfhcJJ·~_; cif BM1~; E•r_;t{ui rement::,. t1eas1.1re111E"!1·1t of r-·ollutar1t concer,tr-atiur1s
[ E: , ( ~)) 1 should be com r:-1 et e d i-1 ti l f 1J r the r, o l .l u t, ants 1 i mite O u r, de,,
P1'et.ruatmt.•nt -;Landard~, (s.i1H:e nur112 2:~ist) but rather for the follow··
i1·1s list of common te::tile waste~ater component-;:
T.s.s.
C,O.[I.
B, 0, D,
Z i r,c
CDPPf:?l'
Chromium
Th~ s t"atemer1t of certification concern ins comr, 1 i a nee or noncor:1P l .i. cl1 ,cc
with star,da1·ds [B,(6)] should be based on con1Pliar1ce with aPPlic3iJl~
local limitatior,s. All other items in sectior, B of the sun1n,ar~
wi 11 1'emain ur1chansed. How~ver, these char1Ses wi'l 1 r1eed tu /J,.:.•
reflected in iterus 6 and 12 of the saruPle BMR,
Fir1all~, the Package cor,tair)s a list of reSulated ir,dust1•j_;~.1
s 1.1L\c3te9ories witt, 0ssociated SIC codes. This li·;::.t is incl 1J 1ied l:.u
he l ,., the F·OTW i dent if~ the sPec if i c I Us reou i r·ed to sut,n, it t, a se l :11 ,;c•
re Ports. This list shou 1 d be cor,s ide red sene r a 1 guidance t1 ec,:; 1.1::: c·
son1e !Us with these SIC codes n1a~ not discl1a,-se wastewater 1'1cJ~,
res u 1 ate d Process while I Us with other ma Jo r SIC codes 1-:1 a•_.:,; : ·1 ~ . ., t: i.::
1-esulated Process as Part of a larger oPeratior),
CoPies of the baseline rePorts should be s 1ibruitt0d L,
Mr. Sal ahd i r, Abd1J l --Han(1.
Supervisor, Pretreatffient Pro31·~;111
M. C. [lep t. NRCD/D iv i ~ion of Er,v i ronmen ta l M ana::u:111...:: 1·1 1
P, O. Bo,: 27687
Ralei!h, N, C, 27611
If ~ou have an~ auestions or con1n,er·1ts ~lease feel free to cal]
me at 919/733-5083,
Sir1cerel'J,
jt(J~M7~
Mack K. Wi.s~ins
F· ,,et rea tffient Te ci"H1 i c i a1·1
~c Salahdin Abdul-Haac1
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Cristex Corporation. Industry Drive. Oxford. N. Carolina 27565. [phone]
Mr. H. T. Ragland
City Manager -Oxford
P. 0. Box 506
Oxford, N. C. 27565
Dear Mr. Ragland:
September 30, 1983
Enclosed please find an Accidental Discharge Prevention Plan
proposed by Cristex Corp. for compliance with Section 2.8 of the
Sewer Use Ordinance.
Upon approval by the City of Oxford, we will begin
construction of containment facilities and implement all sections
of the proposed plan .
WSB/mgo
Enclosure
William S. Bruce
Vice President of Mfg.
CITY OF OXFORD
0 FILE -NO RESPONSE
0 FILE-W/COPY REPLY
REC'D SEP 30 1983 ~ • + u
0 COPY(IES) T1.,
fil-REROUTE TO) h..t-,,f-
0 RESPONSE/ TAPE
--/----··---·-·---··~-·-··----------.. , _____ ---.-~---·---··-·---········----·-···-····--. .,., ______ -.... --------(' .;
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ACCIDENTAL-DISCHARGE
PREVENTION PLAN
CRISTEX CORPORATION
Oxford, North Carolina
September 20, 1983
"Prepared by:
EDI Technology Companies
Post Office Box 16778
GreenviUe, South Carolina 29606 803/292..:1921
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I.
II.
III.
IV.
V.
VI.
··VII.
VIII.
IX.
Executive Summary
General Information
TABLE OF CONTENTS
Spill Prevention Committee
Spill Control Strategy
Potential Spill Sources and Containment
Material Transfer
Spi 11 Response
Area Inspections
Security
Appendix A -DOT Regulations for Loading and
Appendix B -40 CFR Part 117 . Reportable Substances
Appendix C -Internal-Spill Report Forms
Appendix D -· Weekly Spill Control Inspection
Unloading Tank Trucks
Quantities of Hazardous
Checklist
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A.
B.
I. Executive Sunnnary
Facility Description
1 •
2.
3.
4-
5.
Type of facility: Warp knit fabric mill (engaged primarily in knitting, dying, and finishing of flat knit fabrics). Standard Industrial Classification 2258
Location of Facility:
Cristex Corporation
Industry Drive
Oxford, North Carolina Z7565
(919-693-6141)
Located on Industry Drive approximately 1/4 mile West of Highway 15/Industry Drive intersection
Person in charge of facility
Bill Bruce -Plant Manager
Person(s) responsible for Accidental-Discharge Prevention Plan
Bill Bruce -Plant, Manager, Spill Prevention Connnittee Chairman
Marion Munn -Plant Emergency Coordinator
Wastewater Discharge
To city of Oxford, North Carolina, Industrial Wastewater Treatment Plant
Facility Policy/Objectives
This manufacturing facility is committed to provide maximum I · environmental protection by means of the management practices outlined in
this document, and all future revisions of this program. We are aware of I the environmental risks and hazards associated with general textile dying
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and finishing industries, and the specific materials utilized at this
facility. Our policy implies continuing refinement of materials handling
procedures, and spill prevention, response, and control systems by way of
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operations refinement, personnel training, and utilization of available
spill prevention and control technology.
The continuing objective of Cristex Corporation is to responsibily
manage the process facilities to assure minimum effect on the environment
we habitate with reasonable productivity and cost efficiency of operations.
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II. General Information
A. Purpose
The purpose of this Plan is to describe the equipment and procedures
that reduce the probability of an accidental discharge of prohibited
materials to the City of Oxford Industrial Wastewater Treatment Plant.
This Plan is developed in accordance with Environmental Protection Agency
Regulations Title 40, Chapter 1, Subchapter D, Part 112 --"Oil Pollution
Prevention", in acco-rdance iii th EPA-600/9-79-045, "NPDES Best Management
Practices Guidance Document", and in accordance with good engineering
practices'.
B. Availability
The emergency coordinator of the facility for which this Plan is
required should maintain a complete copy of the Plan at the facility. A
copy·of the Plan and any amendments to the Plan must be submitted to the
City of Oxford.
C. Amendments
The owner of this facility is required to amend the Plan for the
following reasons:
1. when required by the City of Oxford after review of the Plan;
2. whenever there is a change in facility design, construction,
operations, or maintenance which materially effects the potential for
an accidential discharge; or
3. the Spill Prevention Committee should review the Plan after each
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spill occurance or at least once every three years, and an amendment
is required if such review indicates more effective control and
prevention technology significantly reduces the likelihood of a spill
event.
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III. Spill Prevention (SP) Committee
A. Responsibilities and· Duties
The SP Committee is responsible for implementing and maintaining a SP
program and will function similarly to a fire prevention or safety
committee. Responsibility and authority is assigned by management for
carrying out management policy and achieving program objectives. Resources
and manpower are .assigned as required. 'rhe Committee ·may typically include
employees from production, engineering, research and development, and waste
treatment. The size and diversity of personnel on the committee reflects
the size and complexity of the plant and the chemicals under consideration.
The committee should advise management on the technical aspects of
environmental incident control but should not impede the decision-making
process for preventing or mitigating spills and incidents.
The main responsibilities of the committee include identification of
materials handled, identification of potential spill sources, establishment
of spill reporting procedures and visual inspections programs, review of
past incidents of spills and countermeasures utilized, coordination of the
activities for spill cleanup, notification to authorities, and
establishment of training and education programs for plant personnel. The
committee has overall responsibility for the program, for reviewing and
evaluating the program, and for instituting appropriate changes at regular
meetings. The committee is also responsible for the necessary review of
new construction and process changes at the facility relative to spill I prevention and control. The committee also evaluates the effectiveness of
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the overall program and makes recommendations to management in support of
corporate policy on spill prevention related matters.
B. Committee Meetings
SP Committee meetings should be conducted in a "parliamentary" manner
to assure systematic review of both new and old business. Minutes should
be recorded and previous minutes read at the beginning of each meeting.
The tentative schedule is for the committee to meet quarterly at the
discretion of the committee. chairman. The committee chairman or a designee
should, as a minimum, review the following topics prior to each meeting to
insure that necessary discussions occur.
1. Meeting minutes.
2. Previous Spill Control Inspection forms.
3. New and outstanding (incomplete corrective actions taken on old
spills) Spill Report forms.
4. Training activities.
c. Committee Organization
Table 1 describes the disciplines that should be represented .in the SP
Committee and is a list of current committee members.
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SP Committee
Title
Chairman
Engineering
Representative
Spill Response
Respresentative
Effective Date __________ , 19 __
Table 1: Spill Prevention Committee Organication
Cristex Individual
Title
Location Phone
Plant Manager Bill Bruce Cristex 919-693-6141
Plant Engr.
Manager Page Hughes Crist ex 919-693-6141
Plant Emergency
Coordinator Marion Munn Cristex 919-693-6141
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IV. Spill Control Strategy
The Oxford facility of Cristex Corporation utilizes a comprehensive
strategy to prevent prohibited materials from reaching the Oxford waste
treatment system. The following is a summary of Cristex's spill control
strategy. A detailed discussion of each aspect of the strategy can be
found in later sections of the report.
A. Material -Transfer Procedures
The transfer of materials from one container to another represents a
potential source of chemical spills. All chemical transfers are covered by
standard operating procedures. These procedures were designed to prevent
accidental employee exposure and release of prohibited materials into the
sewer system. Section VI discusses the procedures for material transfer
operations used at the plant.
B. Inspections
A weekly inspection is made of the facility to identify existing or
potential leaks before they become a problem. Inspection procedures are
discussed in Section VIII.
c. Spill Containment
The facility utilizes diking, and drainage to secure areas to contain
chemicals in the event of a spill. Section V describes the containment
structures and potential spill sources of the facility.
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D. Spill Response
The plant has developed procedures for safely containing and cleaning
up spills. Section VII outlines general and specific response procedures.
E. Other Strategies
These items together with good housekeeping, employee training, and
waste pretreatment enable Cristex to prevent unwanted release of chemicals
from the facility. A Spill Control Committee has been established to
review the practices outlined in this plan to insure that the containment
and countermeasure provisions are effective in preventing spills and
prohibiting spills from impacting the Oxford wastewater treatment system.
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V. Potential Spill Sources and Containment
The potential spill sources at the Cristex Corporation, Oxford
facility, are illustrated in Figures 1 and 2 and described below.
A. Fuel Oil (#6) Storage
Two heated, above ground, No. 6 fuel oil storage tanks are located
outside the northeast corner of the production plant. The tanks have a
30,000 and 20,000 gallon capacity. The tanks are welded steel construction
with pressure type liquid level indicators. At the time of this writing
plans are being developed to place a containment dike around the tanks.
The dike should have the capacity to contain 30,000 gallons plus 5.5 inches
of' free board ( ten year frequency, 24 hour duration rainfall for Oxford,
North Carolina). Rainwater removal from the diked area will be a
supervised procedure, conducted periodically as required. The rainwater
will be inspected for contamination and transferred to the pretreatment
lagoon by pump or gravity flow dependent upon containment structure
design. The fuel oil storage area and associated piping is included in the
inspection format of Section VII of this report.
B. Plant Ventilation Air Pollution Control Devices
Overflow discharges from the rooftop air pollution control devices
flow to the pretreatment lagoon. The wastewater from these units is a
separable (neat) mixture of water and finishing oils. Prior to discharge
to the lagoon the waste passes through a gravity separation tank. The
water is discharged from the bottom of the tank and the oil accumulates on
:
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Oil/Water
Separator
Sanitar sewer
To POTW
Discharge
PretreatmE:nt Lagoon
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-l'igure 2: Oil and Chemical Storage/Use
Areas
Cristex Corporation
Oxford, North Carolina
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' ' ' ' ' ' ' ' ' ' '?'
' To Highway 15
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I ~:
Sanitar sewe
Pr0<;::ess
·i ·7
-.,; . ,:.
.:./.{
-' _;~:
'i"'
-~
'' . ··~::
·•.j;~;
~-~•la ~~~~}: · __ :• ... , .. :::~{-
·,
~ .".'.
.-.:i,
. 'i -:~ 1.~ · · _r;-~~ ' ' ,'tl;,' ~:.r,,
-. }~j\;~
-~~h
' .,~tP'
. ' l.,., .. •..;
" .
,' ~-~·;;-;-
. -~ t
Pretreatm ·
Lagoon:
.r.:
~· ··.._\,; . '
, ;-~~ ... ; "',h,~ "• l J,
· ,'~c ::;\1:;~{f ;:?r~~'~:s~.
: ~-1:~:~}:)\·'
Figure l: Site Plan
Cristex Corporation
Oxford, North Carolina
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top. The tank is inspected periodically to insure clean water discharge to
pretreatment (see Section VIII). The oil is scavanged from the tank as
required.
C. Drum Chemicals
There are no bulk storage facilities for process chemicals on site.
All process chemicals are contained in 55 gallon or less drums. The drums
are transported from the shipping and receiving area to appropriate storage
and use areas within the plant. As indicated by Figures 1 and 2, chemical
storage and use is isolated to the East section of the production building.
the drums remain sealed at the storage sites until ready for use in either
the drug room ( dye mix area), finishing line, or boiler room. Safe
transfer and transport of drummed materials is discussed in Section VI.
Storage areas are inspected in acordance with Section VIII.
D. Normal Process Water Flows
Wastewaters from the various dying and finishing processes within the
plant flow by way of process sewer to the pretreatment lagoon. The lagoon
has a surface area of approximately 1/2 acre and a volume at 5 foot depth
of 0.8 million gallons. The lagoon, when aerators are installed, will
function as an aerated treatment lagoon with approximately 3 days average
hydraulic retention time. The pretreatment system will function as both an
organic removal and waste equalization system. The effluent piping is
designed for subsurface drawoff to prohibit floating oils from entering the
city sewer system. The effluent end of the lagoon will remain unmixed
prohibiting the discharge of solid material which may cause obstruction in
the sewer system.
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Although the lagoon does afford a degree of protection against slug
load discharges to the POTW, process plant operators are reminded that this
is not the lagoons intended use. Periodic analysis of lagoon effluent
quality will permit Cristex personnel to determine if accidental discharges
of prohibited materials occur unnoticed within the process plant. The
I lagoon will be inspected in accordance with Section VIII to assure proper
operation.
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VI. Material Transfer
A. Fuel Oil Transfer
Fuel oil is transferred from tank trucks to the bulk storage tanks at
the tank truck unloading site. Truck delivery routes are confined to Drive
Bas indicated by Figure 1. Tank truck loading/unloading rack procedures
will meet the requirements established by the Department of Transportation
( see Appendix A "DOT Regulations. . • "). The following are general
guidelines that will be followed during each transfer operation:
1 • A qualified Cristex plant operator will be present to control I connect/disconnect operation. The veehicle operator will be present during
the entire transfer operation.
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2. The wheels of the truck will be chocked to prevent movement.
3. Rainwater accumulation will be removed from the diked area
according to guidelines established in Section V.A.
4. Storage tank liquid level will be verified to ensure the tank has
sufficient capacity to receive the fuel oil without overflowing.
5. Flexible hoses will be inspected' for signs of wear prior to
connection.
6. The plant operator will ensure that the connections are correct
and secure before transfer begins. Cam arms on quick connect \I couplings should be wired or taped shut.
\I 7. A warning sign will be provided to prevent vehicle departure
before complete disconnect and final plant operator inspection.
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8. The flexible hoses will be disconnected and the load/unload
line(s) from the storage tanks will then be capped unless in a standby
situation.
B. Drum Transport/Transfer
Drums are inspected by shipping/receiving personnel upon arrival. The
purchasing department is notified if the drums are leaking or otherwise in
poor repair. Drums in satisfactory condition are transported to the appro-
priate storage area. Prior to transport all bungs, venta, and rim seals
are inspected and secured, Drums are transported by fork lift either
individually or in groups of 2-4 on wooden pallets. Two or more drums
transported on a pallet should be fastened together with a strap. Upon
arrival at the storage area the forklift operator should contact the area
supervisor for drum placement instructions.
Drums are moved from the storage areas to use areas with a hand dolly
designed specifically for drum handling, The drums are not opened until
they are placed in use and in most instances are not moved again until
empty. Portable drum pumps are used to transfer liquids from the drum to
the mix tanks. Measuring scoops are used to move powdered dyes from the
drums to mix tanks. After transfer the operator should' inspect the area
for spills before starting another task.
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VII. Spill Response
A. Alert Procedures
Spill response activities are activated immediately upon detection of
an oil or chemical spill. The employee detecting a spill notifies his
immediate supervisor who will confirm the spill and, if necessary, activate
the call tree. Once activated, information should flow quickly along the
tree. If an individual cannot be reached immediately one should continue
calling further along the tree until the information is passed.
In case of a spill that is in danger of release to the environment,
the emergency coordinator or his representative will notify Federal and
State Authorities. State and Federal contacts for oil or chemical spills
are listed below.
The following Federsl and North Carolina state agencies must be
contacted immediately by the emergency coordinator or his representative
for spills that have the potential of environmental release or endangering
public health and safety.
Federal
1. National Response Center
2. EPA Region IV (optional)
North Carolina State Agencies
3. DAY (8 AM -5 PM)
800-424-8802
(24 hr #)
404-881-4062
(24 hr #)
Division of Environmental Management Mr. Ted Mew
919-733-5291
NIGHT
North Carolina Highway Patrol Warning Point 919-733-3861
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City Hall
Day (919/693-5172)
Police Department
Night (919/693-3161
--·---

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EMERGENCY SPILL CONTROL CALL TREE
CRISTEX CORPORATION, OXFORD, NORTH CAROLINA
Spill Observer
Irrcrnediate Supervisor
Emergency Coordinator
Alternates
Emergency Coordinator
Marion Munn
919/693-7142
1. National Response Center
(800/424-8802)
2. Region IV EPA (optional)
(404/881-4062)
3. N. C. Emergency Response
Day (919/733~5291)
Night (919/733-3861)
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Spill Release to Environment
Spill Release
to Oxford
POTW
John Swift
919/693-8892 H 1-----• or
Jim Malenkos
919/693-1262 H
Dee Oakley
919/693-3996 H
Plant Manager
Bill Bruce
919/693-4296
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Page Hughes
919/492-3434
24-Hour Emergency Number
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Potential of Endangering Public
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Fire
Oxford Fire Dept. 693-3311
Emergency Medical Service
Granville Rescue squad 693-5115
Granville Hospital
Police
693-5115
Granville City Sheriff 693-3213
Oxford Police Dept. 693-3161
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FEDERAL LAW REQUIRES THAT THE NATIONAL RESPONSE CENTER BE CONTACTED, and
the plant is responsible for making this contact,
The National Response Center was initiated in January of 1977 to I streamline emergency reporting procedures. The Response Center will
request a minimal amount of information concerning the spill event. The
center will then contact appropriate local authorities who will contact
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Cristex requesting information such as:
1. Name of Company
2, Location of Spill
3, Nature and Potential Danger of the Spilled Material
4,
5,
6.
Volume of Spill
Source of Spill
Time of Spill
7, Anticipated Movement of Spill
8, Action Taken or Anticipated
9, Weather Conditions at Spill
Under Superfund, any release to the environment of 1 lb or designated
quantities under Section 117 of the Clean Water Act shall be reported. The
courts have interpreted "release ·to the environment" to be outside of plant
buildings or spill control areas .. The quantities are listed in Appendix B.
Should an accidental discharge have the potential to impact the City
of Oxford wastewater treatment system, i.e., should a spill enter Cristex's
pretreatment lagoon, the emergency coordinator or his alternate should
immediately notify the c;ty POTW by contacting the City Hall switchboard or
the Police Department.
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Oxford City Hall -Day 919-693-5172
Oxford City Police Department -Night 919-693-3161
The nofification shall include location of discharge, type of waste,
concentration, volume, and corrective actions.
B. Spill Procedures
1. The spill observer will immediately report the detection of a
spill to his supervisor.
2. After confirming the spill, its magnitude, and location, the
supervisor will activate the call tree if in his opinion the spill
cannot be contained and cleaned up with materials and personnel
available to him in his immediate area, or if there is any uncertainty
as to the dangerous characteristics or consequences of the material
spilled.
3. Once the call tree is activated and the emergency coordinator or
an alternate is on-site, he is responsible for coordination of all
spill countermeasure activities.
4-The basic plan of action is to stop spillage, contain, and clean
up the spill before damage occurs. These actions should be conducted
in a safe manner to prohibit personal injury to those involved in
containment and clean up activities, and to insure minimum
environmental inpact.
5. Should the spill be of such magnitude as to require additional
help, the emergency coordinator or his designee, can commandeer
additional on-site employees, call in employees, or request outside
contractors.
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6. Should the spill have potential for release to the environment or
otherwise cause environmental damage the emergency coordinator or his
designee must contact appropriate Federal and State Authorities as per
Section VII.A of this report.
7. Should the spill have potential for entry to the city sewer
system, the emergency coordinator or his designee must contact the
POTW as per Section VII.A of this report.
A useful source of information on spill clean up procedures is
Chemtrec (800-424-9300). Chemtrec is a 24 hour hot line service sponsored
by the Chemical Manufacturers Association designed to give advice on safe
handling of chemical spills. Product name and manufacturer are the key
pieces of information Chemtrec requests.
The following California State Department of Health reprint is
provided as a general guideline for the safe handling of oil and hazardous
material spills.
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Safety Rules for Handling
Oil and Hazardous Material Spills*
*California State Department of Public Health
Bureau of Occupational Health, Berkeley, California
Unidentified Materials
When spilled material is not identified, assume it is hazardous.
1.
2.
3.
4-
5-
1.
2.
3..
4-
5-
DO
Rope off area, or otherwise prevent contact of anyone or anything with
spilled material. If it is a gas, dust or volatile liquid, evacuate
surrounding and downwind areas. If a dust or powder, cover with
canvas, plastic sheets or other material.
Provide first aid, decontaminate with soap and water, remove
contaminated clothing and take anyone affected by the spilled material
to the nearest emergency hospital. Note where they are sent.
In a safe manner, find out what the spilled material is.
Detain vehicle from which spill occurred. Note any contaminated
cargo. Detain persons and property' who have contacted spilled
material.
Report incident to fire, police and health agencies, and ask for
assistance. (Cristex personnel should activate the Emergency Call
Tree.) •
DO NOT
Wash unidentified material off roadway into a waterway or sewer
without official authorization.
Handle leaking container or go into truck van without full protective
clothing and self-contained breathing apparatus.
Walk in spilled material or otherwise contaminate skin, boots,
clothing or vehicles.
Allow vehicles to ride over spill.
Allow anyone to eat or smoke near the spill, or provide source of
ignition.
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1.
2.
3.
1.
2.
Obtain expert
accordingly.
manufacturers
Safety Rules for Handling
Oil and Hazardous Material Spills
Identified Materials
DO
advice on what the hazardous are and deal with them
Health agencies, fire departments and chemical
can provide advice, assistance and infonnation-.
Forward the name of material to the hospital or doctor to which anyone
was sent because tif exposure.
Notify manufacturer of spilled chemical and request services of an
expert decontamination team.
DO NOT
Attempt to clean up any toxic material without adequate protective
clothing and appropriate equipment.
Wash any material into a waterway or sewer without official
authorization.
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c. Reports
If the emergency coordinator determines that the facility has had a
release which could threaten human health, or release to the environment,
he must immediately notify the National Response Center as. described in
Section VII. A.
An internal "Spill Report" form is supplied (Appendix C) and should be
completed within 24 hours of any spill occurance. The purpose of this form
is to evaluate and improve upon spill prevention control and counter-
measures procedures. The Spill Report will be reviewed by the Spill
Control Committee and recommendations to prevent a spill recurrance will be
made. Spill reports and any spill event related correspondence or memos
should be kept on active file a minimum of 3 years.
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VIII. Area Inspections
Potential spill area inspections occur weekly, with the exception of
rainwater accumulation checks on the fuel oil containment area which occurs
daily during wet weather. ·Inspection activities are described by the
checklists supplied in Appendix D. Inspection decrepencies should be
brought to the immediate attention of the Spill Control Committee chairman.
Completed inspection checklists should be submitted to the chairman at the
end of each month and remain on file for three years.
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IX. Security
The facility is fenced and well lighted. A security guard is on duty
seven days per week from 5 p.m. until 8 a.rn. Security personnel are
familiar with the spill alert procedures contained in this plan and will
activate the emergency call tree should problems arise.
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APPENDIX A
DOT Regulations for Loading and Unloading Tank Trucks
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PART 177-CARRIAGE IIY-PUIILIC
HIGHWAY
Subpart &-loading and Unloading
NOTC For prohibited loa.ding and storage
ot hazardous materials, see f 177 .84 8.
§ 177 .834 General rcquittmcnts.
(a) Package3 secured in a vehicle.
Any tank. barrel. drum. cylinder. or
other packaging', not permanently at-
tached to a motor vehicle, which con-
tains any flammable llquld, com-
pcessed gas, corrosive material, poison-
ous material. or radioactive material
must be secured against movement
,au § 177.834
within the vehicle on which It ls being
transported, under conditions normal-
ly incident to transportation.
(b) No hazardOU$ materials on pole
trailen. No hazardous materials may
be loaded Into or on or transported ln
or on any pole trailer.
(c) No smoking while loading or un-
loading. Smoking on or about any
motor vehicle while loading or unload-
ing any explosive. flammable liquid,
flammable solid, oxidizing material. or
flammable compressed gas is forbid-
den.
Cd) Keep fire away, loading and un-
loading. Extreme care shall be taken
in the loading or unloading of any ex-
plosive, flammable llquld, flammable
solid oxidizing material, or flammable
compressed gas into or from any
motor vehicle to keep fire away and to
prevent persons in the vicinity from
smoking lighting matches, or carrying
any flame or lighted cigar, pipe, or
cigarette.
Ce) Handbrake set while loading and
unloading. No hazardous material
shall be loaded Into or on, or unloaded
from, any motor vehicle unless the
handbrake be securely set and all
other reasonable precautions be taken
to prevent motion of the motor vehicle
during such loading or unloading pro-
cess.
Cf> Use of tool!, loading and unload-
ing. No tools which are llkely to
damage the effectiveness of the clo-
sure of P.nY package or other contain-
er, or likely adversely to affect such
package or contalner, shall be used for
the loading or unloading of any explo-
sive or other dangerous article.
Cg) Prevent relative motion between
containers. Containers of explosives,
flammable llqulds, flammable solids,
oxldizlng materials, corrosive· materi-
als, compressed gases, and poisonous
Uqulds or gases, must be so braced as
to prevent motion thereof relative to
the vehicle while In transit. Contain-
ers having valves or other fittings
must be so loaded that there wtll be
the mlnlmum llkellhood of damage
thereto during transportation.
Ch) Precautions concerning contain-
en in tran.sit; fueling road unit.s. Rea-
sonable care should be taken to pre-
vent undue rtse ln temperature of con-
tainers and thelr contents during tran-
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§ 1n.s34
sit. There must be no tampering with
such container or the contents thereof
nor any discharge of the contents of
any container between polnt of origin
B.lld point of bllled destination. Dis-
charge of contents of any container,
other than a cargo tank, must not be
made prior to removal from the motor
vehicle. Nothing contained In this
paragraph shall be so construed a.s to
prohibit the fueling of ma.chlnery or
vehicles used ln road construction or
maintenance.
(1) Attendance requirement.!. Cl)
Loading. A cargo tank must be attend-
ed by a qualified person at all times
when It Is being loaded. The person
Wlio ·ls responsible for loading the
cargo tank ls also responsible for en-
suring that It Is so attended.
(2) Unloading. A motor carrier who
transports he.zardous materials by a
cargo tank must ensure that the cargo
tank Is attended by a qualified person
at all times during unloading. Howev-
er, the carrier's obligation to ensure
·-attendance ·during unloading ceases
when-
(!) The carrier's obligation for trans-
DOrtlng the materials Is fulfllled;
Cll> The cargo tank has been Dlaced
upon the consignee's premises; and
OU> The motive power has been re-
moved from the cargo tan.le ·and re-
moved from the premises.
(3) A person "attends" the Ioacllng
or unloa.dlng of a cargo tank if,
throughout the process, he ls awake,
has an unobstructed view of the cargo
tank. and Is within 7.62 meters (25
feet> of the cargo tank.
<4> A person Is "quall!led"" I! he has
been me.de a.ware of the nature of the
hazardous material which Is to be
loaded or unloaded, he has been In-
structed on the Drocedures to be fol-
lowed in emergencies, he is authorized
to move the cargo tank, and he he.s
the means to do so.
(5) A dellvery hose. when attached
to the cargo tank, Is considered a Dart
of the vehicle.
(j) Prohibited loading combination3
In any single driven motor vehicle or
ln any single unJt of a comb1natlon of
motor vehicles, hazardous materials
shall not be loaded together I! Drohlb-
lted by loading and storage chart.
§ 177 .848. This section shall not be so
Title 49-Trantpor1atlon
construed e.s to forbld the carrying of
materials essential to safe operation of
motor vehicles. (See Motor Carrier
Safety Regulations Part 393 of the
subche.pter.>
Ck) Acce.u to mixed lading&. Flamma-
ble solids, oxidizing materials, or cor-
rosive llqulds, when transported on a
motor vehicle with other lading not
otherwise forbidden, shall be so loaded
e.s to provide ready access thereto for
shifting or removal.
(1) U,e of cargo heater& when tran3-
port!ng certain hazardou.& materiaL
Transportation includes loading, car-
rying, B.lld unloading.
_ (1) When tran3porting expl~&ivel .. :A-
···'•niotor ·vehicle equipped with a··c-argo ·
heater of any type may transport ex-
plosives only if the cargo heater ls ren-
dered Inoperable by: (I) Draining or re-
moving the cargo heater fuel tank:
and (II) disconnecting the heater's
power source.
(2) When tran3parting certain flam-
mable material-Ci> U,e of combu.&tion
cargo heaten. A motor vehicle
equlDped with a combustion cargo
heater may be used to transport flam-
mable llquld or flammable gas only I!
each of the following requirements are
met-
<A> It Is a catalytic heater.
CB) The heater's surface tempera-
ture cannot exceed 130" F. (54" C.>-
elther on a thermostatically controlled
heater or on a heater without ther-
mostatic crintrol when the outside or
ambient temperature Is 60" F. 05.6"
C.) or less.
<C> The heater Is not ignited In a
loaded vehicle.
<D> There Is no name. either on the
catalyst or anywhere in the heater.
· <E> The mB.llufacturer.,has, certl!led--
that the heater meets the require-
ments under DaragraDh (1)(2)(1) of this
section by permanently mark.Ing the
heater "MEETS DOT REQUIRE-
MENTS FOR CATALYTIC HEATERS
USED WITH FLAMMABLE LIQUID
AND GAS."
<F> The heater Is also marked "DO
NOT LOAD INTO OR USE IN CARGO..
COMPARTMENTS CONTAINING
FLAMMABLE LIQUID. OR GAS IF
FLAME IS VISIBLE ON CATALYST
OR IN HEATER."
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Chapter I-Materials Tran1portation Bureau § 177.835
<G> Heater requirements under
§ 393.77 al this title are.complied with.
CID Effective date for combu..stion
heater requirement..,. The requirements
under paragraph (1)(2)(1) al this sec-
tion govern as follows-
(A) Use of a heater manufactured
after November 14. 1975. ls governed
by every requirement under (1)(2)(1) of
this section;
(B) Use of a heater manufactured
before November 15, 1975, ls governed
only by the requirements under
(1)(2)(1) <Al, <Cl, (Dl, <Fl and <G) al
this section until October I, 1976; and
(Cl Use al any heater alter Septem-,·
ber 30, 1976, Is governed by every re-
quirement under paragraph (1)(2)(1) ol
this section.
CUD Re.,trictiom on automatic
carga-3pace-healing temperature con-
trol device.,. Restrictions on these de-
vices have two dimensions: Restric-
tions upon use and restrictions which
apply when the device must not be
used.
CA> Uu re.,lriction,. An automatic
cargo-space-heating temperature con-
trol device may be used when trans-
porting flammable liquid or flammable
gas only if each of the following re-
qulrement.s ls met-
(1 l Electrical apparatus In the cargo
compartment ls nonsparklng or explo-
sion proof.
(2) There ls no combustion appara-
tus in the cargo compartment.
CJ) There ls no connection for return
of alr from the cargo compartment to
the combustion apparatus.
(4) The heating system will not heat
any part of the cargo to more than
130" F. (54" C.).
CS) Heater requtrement.s . .-._· under ..
§ 393. 77 al this t!Ue are complied wlthi
CB) Protection again.st u.se. Flamma-
ble liquid or flammable gas may be
transported by a vehicle, which Is
equipped with an automatic cargo-
space-heating temperature control
device that does not meet each re-
quirement of paragraph (1)(2XIUXA)
ol this section, only It the device Is
first rendered inoperable, as follows-
(1 l Each cargo heater fuel tank, It
other than LPG. must be emptied or
removed.
(2) Each·LPG fuel tank !or automat-
ic temperature control equipment
must have Its discharge valve closed
and its fuel feed li.'1e disconnected.
Cm) Tanks constructed and main-
tained in compliance with spec. 106A
or ll0A <§§ 179.300, 179.301) that are
authorized for the shipment of haz-·
ardous materials by highway in Part
173 of this subchapter must be carried
in accordance with the following re-
quirements:
( 1) Tanks must be securely chocked
or clamped on vehicles to prevent any
shifting.
(2) Equipment suitable for handling
a tank must be provided at any point
. whe:_re a_ tank is to be loaded upon. or
remoVed ·from a vehicle. -· · -·
(3) No more than two cargo carrying
vehicles may be 1n the same combina-
tion of vehicles.
(4) Compliance with§ 174.560 al this
subchapter for combination rail
freight, highway shipments and
§§ 174.532 and 174.533 of this sub-
chapter for trailer-on-flat-car service is
required.
(n) Specl!lcatlon 56 or 57 (§§ 178.251,
178.252, 178.253 al this subchapter)
portable tanks containing .hazardous
materials may not be stacked on each
other nor may any other freight be
stacked on them during transporta-
tion.
(29 FR 18795, Dec. 29, 1964. Redeslgnated at
32 FR 5606, Apr. 5, 1967, and amended by
Arndt. 177-10. 35 FR 1109, Jan. 28, 1970;
Arndt. 177-17, 36 FR 18469, Sept. 15, 1971;
Amdt. 177-1!0, 37 FR 2886, F<b. 9, 1972;
Amdt. 177-21, 37 FR 5950, Mar. 23, ·1972:
Arndt. 177-31, 39 FR 41743, Dec. 2, 197-t;
Arndt. 177-32, 39 FR 45245, Dec. 31, 1974;
Amdt. 177-34, 40 FR 46106, Oct. 6, 1975; 40
FR 49092, Oct. 2, 1975; Amdt. 117-35, 41 FR
16130, Apr. 15, 1976; Arndt. 177-35A, 41 FR
40476,-SepL 20, 1976;,Amdt. 177-37, 41 FR
40(76, SepL 20, 19761
§ 177.835 ExploaiYc&.
<See also§ 177.834 (a) to (kl.)
Ca) Engine stopped. No explosives
shall be loaded Into or on or be un-
loaded from any motor vehicle with
the engine running.
Cb) Care in loading, unloading, or
other handling Q/ e.xplosiva. No bale
hooks or other metal tools shall be
used !or the loading, unloading, or
other handllng al explosives, nor shall
any package or other container of ex•
ploslves, except barrels or kegs, be
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§ 177.835
rolled. No packages o! explosives shall
be thrown or dropped during process
of loading or unloading or handllng of
explosives. Special care shall be exer-
cised to the end that packages or
·other containers containing explosives
shall not catch fire from sparks or hot
gases from the exhaust tailpipe.
( 1) Whenever tarpaulins are used for
covering explosives. they shall be se-
cured by means of rope or wire tie
downs. Explosives placards or mark-
ings required by § 177.823 shall be se-
cured, in the appropriate locations, di-
rectly· to the equipment transpartlng
the e"xploslves. If the vehicle is Pro·-'
vtded with placard boards, the plac-
ards must be applJed to these boards.
(c) Explosives on vehicles in combi-
nalio1L Class A explosives may not be
loaded into or carried on any vehicle
of n combination of vehicles lf:
( 1) More tha.n two cargo carrying V-e-
hicles are in the comblnation;
<2> Any full trailer In the combina-
tion has a wheel base of less tha.n 184
lnches;
(3) Any vehicle In the combination ts
a tank motor vehicle which is required
to be marked or placarded under
§ 177.823; or
(4) The other vehicle In the combi-
nation contains a.ny:
(I) Initiating explosive,
(ti) Packages of radioactive materials
bearing "Yellow Ill" !abets,
(Ill) Class A or B potsons, or
(Jv) Hazardous materials in a porta-
ble tank or a DOT specification 106A
or 110A tank.
(d) [Reserved]
(e) No sharp projectiom imide bodJJ
of vehicle.!. No motor vehicle traru;.
porting. any ldnd of explosive shall
have on the interior of the body in
which the explosives are contained,
a.ny inwardly projecting bolts. screws,
nails, or other inwardly projecting
parts likely to produce damage to any
package or container of explosives
during the loading· or unloading pro-
cess or in transit.
(!) Explosives vehicle.J, fl,oor-3 tight
and lined. Motor vehicles transporting
class A or class B explosives shall have
tight floors; shall have that portion of
the Interior In contact with the load
lined with either non-metallic material
or non-ferrous metals, except that the
Title 49-Tronaportation
llnlng ls not required for truck load
shipments loaded by the Departments
of the Army, Navy or Air Force of the
United · States Government provided
the explosives are of such nature that
they are not liable to leakage of dust,
powder, or vapor which might become
the cause of an explosion. The Interior
of the cargo space must be ln good
condition so that there will not be any
likelihood of containers being dam-
aged by exposed bolts, nuts, broken
side panels or floor boards, or any
similar projections.
(g) No blasti_ng cap, regardless of
· · · tYPe, mO:y be ti-8.IlSported on the same
motor vehicle with any Class A or
Class B explosive unless-
(1) It ts packed In a specification MC
201 (§ 178.318 of thts subchapter> con-
tainer. or
(2) It ts packed and loaded in accor-
. dance with a method approved by the
Department. One method approved by
the Department ls as follows:
Ci) The caps are packed in packag-
ings prescribed In § I 73.66(g) of this
subchapter which 1n tum are loaded
into portable containers or separate
compartments meetlng the require-
ments of the Institute of Makel"S of
Explosives' Standard entitled "!ME
Standard for the Safe Transportation
of Eleetric Blasting Caps In the Same
Vehicle With Other Explosives.'' dated
November 5, 1971 CIME Safety Library
Publication No. 22).
Ch) Lading within bodJJ or covered
tailgaU closed. Except as provided in
paragraphs Cg), <kl. and Cm> of this
seetlon, dealing with the transporta-
tion of llquid nitroglycerin, desensi-
tized liquid nitroglycerin or diethylene
glycol dlnltraie; other than as defined
In§ 173.53(e) of thts subchapter, all of
that_ portion of the lading of any
motor-vehicle which consists of explo-
sives shall be contained entirely within
the body of the motor vehicle or
within the horizontal outline thereof,
without:overhang or projection of any
part of the load and if such motor ve-
hicle has a tailboard or tallgat..,, It
shall be closed and secured ln place
during . such transportation. Every
motor vehicle transporting explosives
must either have a closed body or have
the body thereof covered with a tar-
paulin, and in either event care must
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Chapter I-Material, Transportation Bureau § 177.836
be taken to protect the load from other explosive, or In any quantity ln
moisture and sparks, except that sub-excess of 900 quarts on one motor ve-
jcct to other provlslons· of these rcgu-hicle or 10 quarts In any one lndlvld-
latlons, explosives other than black ual container. Additional quantities of
powder may be transported on flat-bed explosives, other than nitroglycerin.
vehicles If the explosive portion of the desensitized liquid nitroglycerin or
load on each vehicle ls packed in fire diethylene glycol dinltrate. excepting
and water reslstant containers or cov-any type of blasting or percussion cap
erect with a fire and water resist.ant or other detonating device, may be
tarpaulin. carried on such motor vehicle in a
(I) Explosives to be protected against closed or covered bed or body which
damage by other lading. No motor ve-shall be firmly bolted or fastened
hlcle transporting any explosive may above the lid of the compartment con-
transport as a part of Its load any taining the nitroglycerin, desensitized
metal or other articles or materials liquid nitroglycerin or diethylene
.,llkely .to dam1:1.ge such explosive or any glycol dinltrate. _In no case shall the
package in which tt· ls contained, net load be rrio'ie'thaff 7,500 pounds.
wtless the different parts of such load (See paragraph Cm) of this section and
be so segregated or secured In place in spec. MC201 <§ 178.318 of this sub-
or on the motor vehicle and separated chapter).
by bulkheads or other suitable means (I) Separation of tools and supplies
as to prevent such damage~ for preparing charges. Motor vehicles <J> Tra~er of explosives en route. transporting liquid nitroglycerin; de-
No. class A or class B explosive ~ball be. sensitlzed _ _llquid nitroglycerin or dieth-
tr8.nsferred from one coritB.lner ·to a.n·_.--.--Ylene glycol dinltrate, may also trans-
other, or from one motor vehicle to port the tools and supplies necessary
another vehicle, or from another vehl-for preparing and firing charges there-
cle to a motor vehicle, on any public of: Provided, That such tools and sup-
hlghway, street, or road, except in case plies be properly secured in place so as
of emergf!ncy. In such cases red elec-to prevent their coming in contact
tric lanterns, red emergency reflectors with the body above speclfled.
or red flags shall be set out in the <m>·Caps or other explosives. Any ex-
manner prescribed for disabled or plosive, including desensitized llquld
stopped motor vehicles. <See Motor explosives as defined in § 173.53(e) of
Carrier Safety Regulations, Part 392 this subchapter. other than liquid nl·
of this subchapter.) In any event, all troglycerln. desensitized liquid nltro•
practicable means, in addition to these glycerin or dlethylene glycol dlnltrate,
herelnbefore prescribed, shall be transported on any motor vehicle
taken to protect and warn other users transporting liquid nitroglycerin. de•
of the highway against the hazard In· sensitized liquid nitroglycerin or dleth-
volved in any such transftr or against ylene glycol dlnltrate, must be segre-
the hazard occasioned by the emergen-gated, each kind from every other
cy making such transfer necessary. kind, and from tools or other supplies.
__ Ck) Loading requiremenU.Jo_r _liquid Bl~ting caps must be packed in specl-
nitroglycerin, d.e.,en.,itized liquid ni• llcatlon MC 201 <§ 178.318-o'!·thls sub-
troglycerin,, or diethylene glycol dini-chapter) containers.
trate. Llquld nitroglycerin, desensl•
tlzed liquid nitroglycerin, or dlethY·
lene glycol dlnltrate. other than as de-
fined In § 173.SJ<e> of this chapter,
may be accepted for transportation
and transported only by motor carrl·
ers other than common carriers ll It be
loaded into or on a truck having the
type of body specllled In spec. MC200
(§ 178.315 of this subchapter). No
liquid nitroglycerin. desensitized liquid
nitroglycerin or dlethylene glycol dlnl·
trate may be loaded directly above any
[29 FR.18795, Dec. 29, 1964. Redeslgnated at
32 FR 5606. Apr. S, 1967, a.nd amended by
Amdt. 177-17, 36 FR 18469. Sept. 15, 1971;
Arndt. 177-22. 37 FR 21531, Oct. 12, 1972;
Amdt. 177-31, 39 FR 41743, Dec. 2, 1974;
Arndt. 177-35, 41 FR 16130, Apr. 15, 1976) ·-. ' .. ·,
§ 177.836 Nonexplosive material
Ca) No restrictions are prescribed In
Parts 170-189 of this subchapter for
the packing. handling. and transporta•
tlon of material relating to ammunl·
tlon for cannon, but contalnlng no ex-
549
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§ 177.837
plosive or other dangerous article,
such as cartridge cases, "dummy" or
"drill" cartridges, etc .. sand.loaded pro-
Jectlles, sand-loaded bombs. empty
projectiles, empty mines, empty
bombs, solid proJectJJes, or empty tor-
pedoes. Rotating bands should be pro-
tected cgalnst deformation by method
of packing or loading.
[29 FR 18795, Dec. 29, 1964. Redeslgnated a.t
32 FR 5606, Apr. 5, 1967, a.nd amended by
Arndt. 177-35, 41 FR 16130, Apr. 15, 19761
§ 177.837 Flammable liquids.
<See also§ 177.834(al to (kJ.J
Ca) Engine !topped. ·Unless the
engine of the motor vehicle Is to be
used for the operation of a pump, no
flammable llQuld shall be loaded Into,
or on, or unloaded from an)' motor ve-
hicle while the engine Is running.
Cb) Bonding and grounding contain-
ers other than cargo tank3 prior to and
during tran.s,fer of lading. For contain-
ers which are not 1n metallic contact
with each other, either metallic bonds
or ground conductors shall be pro-
vided !or the neutralization of possible
static charges prior to and during
transfers of flammable llQu!ds be-
tween such containers. Such bonding
shall be made by Clrst connecting an
electric conductor to the container· to
be lilied and subsequently connecting
the conductor to the container from
which the IIQuld Is to come, and not ln
any other order. To provide against ig-
nition of vapors by discharge of static
electricity, the latter connection shall
be made at a point well removed from
the opening from which the flamma-
ble llQu!d Is to be discharged.
(c) Bonding and grounding cargo
tanks before and during tran.!{fer-of
lading. < 1) When a cargo tank is
loaded through an open fllling hole,
one end of a bond wire shall be con-
nected to the stationary system piping
or Integrally connected steel framing,
and the other end to the shell of ·the
cargo tank to provide a continuous
electrical connection. (IC bonding Is to
the framing, It Is essential that piping
and framing be electrically lnten:on-
nected.) This connection mU.St be
made before any Cll!lng hole Is opened,
and must remain ln place until alter
the last Cllllng hole has been closed.
Additional bond wires are not needed
Title 49-Transportation
around AB-Metal flexible or swivel
Jolnt.s, but are required for nonmetal-
lic flexible connections in the station-
ary system piping. When a cargo tank
is unloaded by a suction-piping system
through an open filling hole of the
cargo tank, electrical continuity shall
be maintained from cargo tank to re-
ceiving tank.
(2) When a cargo tank is loaded or
unloaded through a vapor-tight (not
open hole) top or bottom connection,
so that there ls no release of vapor at
a point where a spark could occur.
bonding or grounding, ls not required.
Contact.of the):iosed connection must
be made before flow starts and must
not be broken until after the flow ls
completed.
(3) Bonding or grounding ls not re-
quired when a cargo tank ls unloaded
· through a nonvapor-tight connection
into a stationary tank provided the
metallic C!lllng connection Is main-
tained ln contact with the C!lllng hole.
(d) Pyroforic liquid.! in cylinders.
Cylinders containing pyro!orlc liquids,
n.o.s .• unless packed in strong wooden
boxes and secured therein to protect
valves. must be loaded with all valves
and safety relief devices ln the vapor
space, and must be secured so that no
shifting will occur ln trans! t.
(e) Manholes and valves cloud.. A
person shall not drive a tank motor ve-
hicle and a motor carrier shall not re-
quire or penn.Jt a person to drive a
tank motor vehicle containing a flam-
mable llQu!d (regardless of Quantity)
unless-
( 1) All manhole closures on the
cargo tank are closed and secured; and
(2) All valves and other closures in
liquid d1scha.rge·-·systems are·.-.-closed
and Cree o( leaks.
[29 FR 18795, Dec. 29, 1964, as amended by
Order 66, 30 FR 5748, Apr. 23, 1965. Rede-
slgnated at 32 FR 5606, Apr. 5, 1967, and
amended by Arndt. 177-16, 36 FR 10785,
June 3; 1971; Arndt. 177-31, 39 FR 4174.3, ..
Dec. 2, 1974; AmdL 177-37, 41 FR 40476,
Sept. 20, 1976 J
§ 177.838 Flammable solids and oxidizing
matcriali..
<See also§ 177.834 (al to (k)).
Ca) La.ding within bodv or covered;
tailgate closed; pick-up and deliveTJI.
All of that portion of the lading of any
550
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Chapter I-Materials Transpor1ation Bureau § ln.838
motor vehicle transportlng flammable
sollds or oxldlzlng lllaterlals shall be
contained entirely within the body of
the motor vehicle and shall be covered
by such body. by tarpaulins, or other
suitable means, and I! such motor ve-
hicle has a tailboard or tallgate, it
shall be closed and secured 1n place
during such transportation: Provided,
however, that the provisions of this
paragraph need not apply to "pick-up
and delivery" motor vehicles when
such motor vehicles are used in no
other transportation than ln and
about cltles, towns,, or villages. Ship-
ment of Phosphorus pentasul!lde in
tightly closed DOT Speclflcatlon 56
metal portable tanks need not be cov-
ered by a tarpaulin whlle being trans-
ported on flat bed motor vehicles.
(b) Article, to be kept drv. Special
care shall be taken in the loading of
any motor vehicle with flammable
solids or oxidizing materials which are
ltkely to become hazardous to trans-
port when -wet.· 'to keep them from-·
being wetted during the loading pro-
cess and to keep them dry during tran-
sit. Special care shall also be taken in
the loading of any motor vehicle with
flammable solids or oxidizing materi-
als, whtch are llkely to become more
hazardous to transport by wetting, to
keep them from being wetted during
the loading process and to keep them
dry during transit. Examples of such
dangerous materials are charcoal
screenings, ground, crushed, or pulver-
ized charcoal. and lump charcoal.
Cc) Lading ventilation. precaution.,
again.st spontaneous combu.stioTL
Whenever a motor carrier has knowl-
edge concerning the hazards of _spon-
taneous com bus ti On· or hetitlng O"! any
article to be loaded on a motor vehicle,
such article shall be so loaded as to
afford sufficient ventilation of the
load to provide reasonable assurance
against fire from this cause; and In
such a case the motor vehicle shall be
unloaded as soon as practicable after
reaching lt.s destination. Charcoal
screenlngs1 or -ground, crushed, granu-
lated. or pulverized charcoal. In bags.
shall be so loaded that the bags are
laid horizontally 1n the motor vehicle,
and so piled that there will be spaces
!or effective air circulation, which
spaces shall not be less than 4 ~ches
wide; and air spaces shall be main-
tained between rows o( bags. Bags
shall not be piled closer than 6 inches
from the top of any motor vehicle
with a closed body.
<d) Loose or baled nitrate of soda
bags. Loose or baled unwashed, empty
bags, having contained nitrate of soda,
may be transported in truck.load lots
only in motor vehicles, and such motor
vehicles must have closed or covered
bodies lined with paper; such ship-
ments are required to bC loaded by the
shipper and to be unloaded by the con-
signee. "<e> ··stii"iifng· or blocking-of packages
of matche3. Special care shall be exer-
cised In the Joe.ding of packages con-
taining "strike-anywhere" matches to
prevent the shifting or Jamming of
any such package during transit. To
this end, the packages shall be com-
pactly loaded with the strongest di-
mensions o( each box or other contain-
er loaded lengthwise of the motor ve---hlcle.-,
C 1) Smooth vehicle interior for
matche3. Unless strike-anywhere
matches are contained in wooden out-
side boxes, special care shall be taken
to provide that the inside surfaces of
any motor vehicle into which such
matches are to be loaded and with
which surfaces the containers might
come in contact, shall be smooth,
without protrusions of any sort. such
as bolts, nuts. sharp edges, or corners,
etc., and there shall be provided for
this purpose smooth wooden inner lin-
ings. If the Interior of the motor vehi-
cle is not otherwise smooth ln accor-
dance with this requirement.
(2) Flammable liquid,. Matches
must not be loaded neXt• to a package
bearing a flammable liquid label.
(f) Nitrates. except ammonium ni-
trate having organic coating. listed In
§ l 73.182(b) must be loaded In closed
or open type motor vehicles, which
must be swept clean and be free of any
projections capable of Injuring bags
when so packaged. When shipped ln
open typemotor vehicles, the lading
must be sultably covered. Ammonium
nitrate having organic coating must
not be loaded In all-metal vehicles.
other than those me.de of aluminum
or alumlnum alloys of the closed type.
<See§ 177.823 (aX4) and (5).)
551
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§ 177.839
(g) Smokeless powder for small arms In quantities not exceeding 100 pounds net weight transported in one car or motor vehicle may be classed as a flammable solid when approved tor this classification by the Bureau of Explosives. Maximum quantity In any
inside packaging must not exceed 8 pounds and Inside packagings must be arranged and protected so as to pre-vent simultaneous Ignition of the con-tents. The complete package must be a type approved by the Bureau of Ex-plosives. Each outside packaging must
bear a flammable solid label.
(29 FR 18795: oe<:. 29, fga4: Redes"ign~U:-ct··at.
32 FR 5606, Apr. 5, 1967, and a.mended by Arndt.. 177-24, 38 FR 5315, Feb. 27, 1973; Arndt. 177-38, 42 FR 11241, Feb. 28, 1977]
. § 177.839 Corroeive liquids.
(See also§ 177.834 (a) to <kl.)
(a> Nitric acid.. In addition to the re-quirements set forth in paragraph (b) of this section no carboy or other con-tainer of nitric acid shall be loaded
above any container containing any other klnd of material. The loading of carboys or other containers of nitric acid shall be limited to two tiers high. Cb) Carboy! and frang-ible contain-en. In general, individual carboys and frangible containers of corrosive liq-uids, including charged electric storage batteries. must. when loaded by hand, be Individually loaded Into and un· loaded from any motor vehicle in which they are to be, or have been,
transported. All reasonable precau-
tions must be taken to prevent, by all practicable means. the dropping of any such containers or batteries con-taining corrosive liquids. No such con-tainer or battery may be loaded into a motor vehicle having an uneven floor surface. It shall be pennlsslble to load on or transPort ln any motor vehicle any authorized carboys or frangible shipping containers, containing corro-sive UquJds, more than one tier high above any floor only l! such carboys or other containers are boxed or crated, or are ln barrels or kegs, as required by Parts 170-189 of this subehapter.
and only lf such containers are so stacked that the weight of each tier above the first Is entirely supported by the boxes, crates, barrels, kegs, or other authorized means of enclosing
Title 49-Tran1por1ation
the carboys or frangible containers. Only so many tiers as may adequately
be so supported without danger of crushing or breaking, shall be pennlt·
ted. Means must be provided to pre•
vent by all practicable means. in all
cases, the shifting of containers or bat-
teries during transit. Nothing con-
tained in this section shall be so con-strued as lo prevent the use of cleats or other retaining means !or the pur-pose of preventing shifting of contain-ers or batteries. For the purposes of this section a false floor or platform. secured against relative motion within the body of the motor vehlcle:'"Shau be deemed to be a floor. <For recommen· dations for handling leaking or broken packages, see§ !77.858(a).J
cc> Storage batteries. In addition to the requirements set forth 1n para-graph Cb) of this section, all storage
batteries containing any · electrolyte
shall be so loaded, I! loaded with other lading. that all such batteries will be protected against other lading falling onto or against them; and adequate
means shall be provided 1n all cases for the protection and Insulation of · bat-tery terminals against short circulL5.
Cd) Corrosives in cargo tanks. A person shall not drive a tank motor ve• hlcle and a motor carrier shall not re-quire or permit a person to drive a tank motor vehicle containing corro-sives <regardless of quantity) unless-
< 1 > All manhole closures on the cargo tank are closed and secured: and (2) All valves and other closures ln
liquid discharge systems are closed
and free of leaks.
(29 FR 18795, Dec. 29, 1964. Rede.signaled at 32 FR 5606, Apr. 5, 1967, and amended by . Arndt. 177-21, 37 FR 5950, Mar. 23, 1972; Arndt. 177-31, 39 FR "-174.3, Dec. 2, 1974;
Arndt. 177-35, -fl FR 16130, Apr. 15, 1976;
Arndt. 177-37, 4.1 FR 40476, SepL 20, 1976]
§ 177.840 Compressed guea.
<See also§ 177.834 (al to. (kl.J
ca> Floon ·or plat.forih.s esseii.tiaUV
fl.at. Cylinders containing compressed
gases shall not be loaded onto any part of the floor or platform of any motor vehicle which ls not essentially
flat; cylinders containing compressed
gases may be loaded onto any motor
vehicle not having a floor or platform
only U such motor vehicle be equipped
552
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Chapter I-Material, Tranaportation Bureau §177.841
with suitable racks having adequate
means for securing such cylinders ln
place therein. Nothing contained In
this section shall be so construed as to
prohibit the loading o! such cylinders
on any motor vehicle having a floor or
platform and racks as herelnbefore de-
scribed.
< 1 > Cvlinder1. To prevent their over-
turning, cyllnders containing com-
pressed ·gases must be securely lashed
in an upright position; loaded into
racks securely attached to the motor
vehicle packed 1n boxes or crates of
such dimensions as to prevent their
overturning; or loaded ln.JL_hor_izontal
position. Specification i:JOT~4L cylin-
ders must be loaded 1n an upright posi-
tion and securely braced.
(2) Cl/linden for liquefied hydrogen.
Specification DOT-4L cylinders con-
talnlng liquefied hydrogen must be
transported only on motor' vehicles
with open bodies which are equipped
with suitable racks or supports having
clamps or securing bands capable of
holding the cylinders upright when
they are subjected to an acceleration
of at least 2 ••g•• In any horizontal di-
rection.
(I) The combined total of the hydro-
gen venting rates as marked on the
cylinders on one motor vehicle must
not exceed 60 standard cubic feet per
hour.
(ii) Motor vehicles loaded with cylin-
ders containing lique!led hydrogen
may not be driven through tunnels.
<ill) Highway transportation is limit-
ed to private and contract motor carri-
ers only and to direct movement from
point of origin to destination.
Cb) Portable tank containers contain-
ing compressed gases shall be loaded
on motor vehicles only~ follows:
(1) Onto a flat floor or platform of a
motor vehicle.
(2) Onto a suitable frame of a motor
vehicle.
(3) In either such case, such contain-
ers shall be safely and securely
blocked or held down to prevent move-
ment relative to each other or to the
supporting structure when in transit,
particularly during sudden starts and
stops and changes o! direction o! the
vehicle.
(4) Requirements of subparagraphs
Cl) and (2) of this paragraph shall not
be construed as prohibiting stacking of
containers providtd the provisions of
subparagraph (3) of this paragraph
are fully complied with.
Cc) (Reserved}
Cd) Engine to be stopped in tank
motor· vehicles, except for transfer
pump. No flammable compressed gas
shalI be loaded into or on or unloaded
from any tank motor vehicle with the
engine running unless the engine ls
used tor the operation of the transfer
pump of the vehicle .. Unless the deliv-
ery hose ls equipped with a shut-off
valve at Its discharge end. the engine
o! the motor vehicle shall ·be stopped
at the finish of such loading or un-
loading operation while the filling or
discharge connectioflS are disconnect-
ed.
Ce) Chlorine cargo tanks shall be
shtj:,ped only when equipped (1) with a ___ .
gas mask of a type approved by the
U.S. Bureau of Mines !or chlorine ser-
vice: <2> with an emergency kit for
controlling leaks in fittings on the
dome cOver plate.
(!) No chlorine tank motor vehicle
used for transportation of chlorine
shall be moved, coupled or uncoupled.
when any loading or unloading con-
nections are attached to the vehicle.
nor shall any semi-trailer or trailer be
left without the Power unit unless
such semi-trailer or trailer be checked
or equivalent means be provided to
prevent motion.
(g) Each liquid discharge valve on a
cargo tank, other than an engine fuel
line valve, must be closed during trans-
. Portation except during loading and
unloading.
(29 FR 18795, Dec. 29, 1964. Redeslgne.ted at
32 FR 5606, Apr. 5, 1967, and amended by
Arndt. 177-5, 34. FR 7162, May 1, 1969;
AmdL 177-10, 35 FR 1110, Jan. 28, 1970;
AmdL 177-28, 38 FR 27598, Oct. 5, 1973;
.b.mdt. \77-37, 41 FR 404.76, SepL 20, 1976]
§ 177.841 Poisons.
<See also§ 177.834 Ca) to Ck).)
(a) A rsenical compound.3 in bulk.
Care shall be exercised in the loading
553
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§ 177.842
and unloading of "arsenlcal dust", "ar-
senic trioxide", and "sodium arse-
nate", allowable to be loaded Into sift-
proof. steel hopper-type or dump-type
motor-vehicle bodies equipped with
water-proo(, dust-proof covers welJ se-
cured in place on all openings, to ac-
compllsh such loading with the mini-
mum spread of such compaunds lnto
the atmosphere by all means that are
practicable: and no such loading or un-
loading shall be done near or adjacent
to any place where there are or are
likely to be, during the loading. or un-
loading process a.sseinbI3.ges·ot persons
other than those engaged In the load-
ing or unloading process, or upon any
public highway or in any public place.
(1) The motor vehicles must be
marked· '·-· · tjr~-· ·"'accordance with
§ l 73.368(b) of this chapter.
(2) Before any motor vehicle may be
used for transporting any other arti-
cles, all detectable traces of arsenlcal
materials must be removed therefrom
by flushing with water, or by other ap-
propriate method, and the marking re-
moved.
Cb) No Class A or irritating materials
in cargo tanks. No poison, Class A, or
Irritating material may be loaded into
or transparted in any cargo tank.
Cc) Cla.u A poi.soru or irritating ma-
terial.$. The transportation of a Class
A poison or an Irritating material is
not permitted If there ls any intercon-
nection between packagings.
(d) Poiloru in cargo tank.s. A person
shall not drive a tank motor vehicle
and a motor carrier shall not require
or perm.it a person to drive a tank
motor vehicle contain'iiig· ·POisons (re-
gardless of quantity) unless-
( l) All manhole closures on the
cargo tank are closed and secured; and
(2) All valves and other closures in
liquid discharge systems are closed
and free of leaks.
<e> A carrier may not transport a
package bearing a poison label in the
same transport vehicle with material
that is marked as or known to be food-
stuff, feed or any other edlble material
Intended for consumption by humans
or animals.
Title 49-Tran,portation
[29 FR 18795, Dec. 29, 1964. Redeslgnated at
32 FR 5606, Apr. 5, 1967. and amended by
Arndt. 177-5. 34 FR 7163, May 1. 1969;
Arndt, 177-9, 34 FR 18554, Nov. 21, 1969;
Arndt. 177-10, 35 FR 1110. Jan. 28, 1970;
Arndt. 177-24. 38 FR 5315, Feb. 27, 1973;
Amdl. 177-31, 39 FR 41743, Dec. 2. 1974;
Arndt. 177-35, 41 FR 18130. Apr. 15, 1976;
Arndt. 177-37, 41 FR 40476. Sept. 20, 19761
§ 177.842 Radioactive material.
(a) The number of packages of radio-
active materials In any motor vehicle,
trailer. or storage location must be
limited so· that· the ··tota1-,~tral1Sport.-:-
index number. as defined in
§ 173.389(!) of this subchapter and de-
termined by adding together the
transport index numbers on the labels
of the individual packages, does not
exceed 50. This provision ·ctoes not
apply to exclusive use shipments de-
scribed in § 173.3930>. 173.396Cf>, or
173.392 of this subchapter.
Cb) Packages of radioactive material
bearing "radioactive yellow-II" or "ra-
dioactive yellow-Ill" labels must not
be placed in a motor vehicle or in any
other place closer than· the distances
shown in the following table to any
area which may be continuously occu-
pied by passengers, employees, oi-ship~
ments o! animals, nor closer than the
distances shown in the table below to
any package containing undeveloped
film (if so marked). If more than one
of these packages is present. the dis-
tance shall be computed from the fol-
lowing table on the basis of the total
transport lndex number (determined
by adding together the transpart
index numbers on the labels of the in-
dividual packages) or packages in the
vehicle or storeroom. Where.-. more
than one group of packages is present
in any single storage location. a ·single
. group may. not have a total transport
index greater than 50. Each group of
pa.ckages··must be handled and ·stowed
not closer than 6 meters (20 feet>
(measured edge to edge) to any other
group.
Cc> Shipments of low speclf!c activity
materials, as defined in § 173.391 of
this subchapter, must be loaded so as
to avoid spillage and scattering or
loose materials. Loading restrictions
554
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Chapter 1-Materlala Transportation Bureau § 1n.s43
are set forth In § 173.397 of this sub-
chaptcr.
(d) Packages must be so blocked and
braced that they cannot change posi-
tion during conditions normally inci-
dent to transportation.
Mlnlmum
dllt.&nce In
feet to area
Mlnlmum a.epuatlon distances 1n feet or persona. or to neucst undeveloped film for va.rtow mlnlmum Tot&l triuuPOrt Index
None ___________ _
0.1 to 1.0 __________ _
I.I to 5.0:-----------
U to 10.0:----------10.1 to 20.0 _________ _
20.l to 30.0 _________ _
30.1 to 40.0 _________ _
40.l to 50.0
Up to 2
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Non: 1: The distance 1n thr. table must be
measured !rom the nearest point on the
pacta.ges ot radioactive materials.
(e) Persons should not remain un•
necessartly ln a vehicle contalntng ra•
dloactlve materials.
(l) Each fissile class III radioactive
material shipment (as defined In
§ 173.389(a)(3) of this subchapter)
must be transported in accordance
with one of the methods prescribed In
§ l 73.396(g) of this subchapter. The
transport controls must be adequate to
assure that no fissile class III ship.
ment Is transported In the same trans-
port vehicle with any other fissile ra-
dioactive material shipment. In load-
ing and storage areas ea.ch fissile class
III shipment must be segregated by a
distance of at least 20 feet from other
packages required to bear one of the
"Radioactive·• labels described In
§ 173.416 of this subchapter.
[Amdt. 177-3, 33 FR 14933, Oct. 4, 1968;·33
FR 19823, Dec. 27, 1968; Amdt. 177-23, 38
FR 4399, Feb. 14, 1973; 38 FR 5315, Feb. 27,
1973; AmdL 177-32, 39 FR 45245, Dec. 31,
1974; Amdt. 177-35, 41 FR 16131, Apr. 15,
1976; Amdt. 177-37, 41 FR 40476, Sept. 20,
19781
§ 177.843 Contamination of Tehicl«.
(a) Each motor vehicle used for
transporting low specific activity ra-
llmca of tn.nalt di.st.a.nee In
feet from
dlvldln1
pa.rtlllon of
2-• •-• 8-12 Over 12 CU'fl'O com-hours houni houn houn partment.a
0 0 0 0 0 , J ' • 1 • ' ' 11 2
' • 11 15 J • 12 1, " ' ' 10 15 20 " • 11 17 " lJ ' 12 10 ,. " 7
ctioactlve materle.ls 1n truckload lots
under the provisions of § l 73.392(d) of
this subchapter must be surveyed with
appropriate rad.Jatlon detectlOn IIlSfru-
ments after each use. Carriers must
not return such vehicles to service
until the radiation dose rate at any ac-
cessible surface ls not more than 0.5
mllllrem per hour. and there ls no slg-
nlflcant removable rad.Joactlve surface
contamination (see § 173.399 of this
subchapter).
(bl This section does not apply to
any vehicle used solely for transport-
Ing radioactive material ll a survey of
the Interior surface shows that the ra-
ctiatlon dose rate does not exceed 10
mllllrem per hour at the interior sur-
face or 2 mllllrem per hour at 3 feet
from any interior surface. These vehi-
cles must be stenciled with the words
"For Radioactive Materials Use Only"
In lettering at least 3 Inches high In a
conspicuous place, on both sides of the
exterior of the vehicle. These vehicles
must be kept closed at all times other
than loading and unloading.
Cc) In case of fire, accident, break-
age, or unusual delay involving ship-
ments of radioactive material, see
§ 177.861.
[Arndt. 177-3, 33 FR 14933, Oct. 4, 1968, as
amended by AmdL 177-35, 41 FR 16131,
Apr. 15, 19761
555
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APPENDIX B
40 CFR Part 117 .•• Reportable Quantities of Hazardous Substances
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S-522
131:2051
ENVIRONMENTAL PROTECTION AGENCY REGULATIONS ON
DETERMINATION OF REPORTABLE QUANTITIES FOR
"HAZARDOUS SUBSTANCES
(40 CFR 117; 44 FR 50776, August 29, 1979, Effectire September 28, 1979;
Corrcc(cd by 44 FR 58711, October 11, 1979; 44 FR 58910, October 12, 1979; 44 FR
65400, Norrmbcr 13, 1979)
(Editor's note: EPA August Z9, .[979
indelinilcty deCcrrcd the cClecUvc d.ttc of
these regulations Cor common carriers
who arc precluded by Cederal law Crom
obtaining data on whether their cargoes
include haz.ardous substances ( (4 FR
S07661_:· EPA September 17, 1980, said
that common cacriers will be required Lo1
report dischare:es of har.ardous sub--
stances beginnang November 20. 1980
(◄S FR 61617).
Moreover, promulgation o( this part
c((cctively IHts the Federal Maritime
Commission's stay or 9:pplicable pro-
visions of (6 CFR SU. pertaining to
financial liability Cor discharges o(
haz.ardous substances. The commission•s·
rules have the same effective date as
this part. (Sec editor's riotc al end of (6
CF'R S42, published al page Ill: 1101.I
EPA September 17, 1979, postponed
applicability and enlorcement o( these
regulations for lime, pending rir\al action
regar.ding the continued designation o(
c·atcium ox:ide and calcium hydroxide as
hazardous substances ((( F'R 53749),
The agency November 13. 1979. deleted
these chemicals from the hazardous sub--
st.lnces list. I
PART 117-0ETERMINATION OF
REPORTABLE au·ANTITIES FOR
HAZARDOUS SUBSTANCES
Sub'part ·A-C•n•ul· Provl■lon■
;;.<-
I 11.1 Dcllnlllo•,..
11:.2 A.bhor•Yiatlons.
111.l o.,,.,,....ln•II°" o( rcr-••bl•
quarnhics,
Subp.art ~AppffcablUty
tt='.11 Ccncr.11 applic•hili1y.
tt7.1Z Appticvbility 10 dischargc1 rrom
focilitic, with NPOES pcrmils.
117.tl Ap,plkuhiH1y to discharges from
publicly-owned treatment work1 and
!heir uscn ..
117.U pc~_o_os_tr.11ion projccu.
Subpart-C-NoUee of Dbch.■rg• of III work• u defined by 1ec1'on ZIZ of the
Rcport>blc OuantJty Act. which It owned by• State or
ttf.%1 Notice. municipaHty (as defined by 1ecl10n
·117.u · Peultle ■• SOZ(4) o( the Act). This definition
117~ Uabilitics for nmoval includes .any sewers that convey
. ~':'1hori1y: Sccs. 311 and SOt(■l. reder•l. . . .. _ .. wastewater to such a treatment works
Water !'ollu1io~ Control Act ~33 US.C. 1ZS1·cl .. : --~·but does not include pipes·:· sewe"rs or •
,cq.J. ( thc:,\cl J and Exccuhve Order 11735. other conveyances not connected lo a
SUb)l~rt·.s:..:.:cencral Profrilons facility providing lrealmenl. The term
· · also means the.munkipatily as deftncd
1.117.1 Definitions. in section 502( 0. o( the Act~ which has
As us~d in this part. all lehns shall jurisdiction over the indirect discharges
haVe the meanings staled in ,co·CFR Part lo and the discharges Crom such .a
UG. treatment works. ·
(a) .. Reportable quantities .. means (g) "'Remove0 or .. removal" refers
quantities that may be hannCul as set. to removal o( the oil or haurdous
forth in I 117.3. the discharge o( which is substances Crom the waler and shoreline
■ violation of section 31 l(b)(J) and or lhC taking of such other action$ as
requires notice as set forth in I 117.21. may~ necessa.ry·to minimize Or
(b) "Administrator" means the mitigate ~am•~• to the public heal_lh or
Administrator o( the Environmental ·welfare. mcludmg, but not limited to,
Protection Agency ("EPA"). Cish, shellrish, wildliCc, and public and
.(cl .. Mobil& sou·rce" means any private property. shorelines, and beaches.
vehicle. rolli.ng stock. or other means o(
transporta1tion which contains or'carries
a report3ble quantity o( a hazardous·.
substance.
(di "Public record" means the NPOES
pennit application or·the NPDES permit
itself and the ""record Cot final pCrmit" as
defined in 40 CFR lZUZZ.
(el .. National Pretreatment Standard" .
or· .. Pretreatir1C'nt Standard~:mc·anS any::2:--·
regulation containing pollutant
discharge limits prom.ulg:ited by the EPA
In accordance witlr aection 307 (b) and
(c) of lhc Act, which applies to
induslri.11 users or a publicly owned
treatment works. It (urther means any
State or local pretre:itmcnt requirement
:1pplicablc to a discharge and which is
incorJ)oratcd into a pennit issued lo•a
publicly owned treatment works under
section 40Z of the /\ct.
(0 ""Public!~• Owned ~reatment
\Voeks-or ··roTW·· means a trc.1tment
Ch) '"Contiguous zone"' means the
entire. zone established by the Uniled
Slates under Article Z( or the
Convention on the Territorial Sea and
Contiguous Zone.
(i) ""Navigable waters .. ffle:1ns .. w .. ters
of th_e United States. including the.
territorial seas."" Thia tenn includes:
(1) All.waters .,.,tii.c;_h arc eum:nlly
use<L i-fere used U1 the put. or.may be
,usceplil.tle to uae [,n interstate or for,t:ign
commerce. including all waters which
are subject to the ebb and flow of the
tide:
(Z) Interstate wale.-.. including
interstalc wetlands:
{:l) All other waten ~uch es intrastute
lakes. rivers. streams. (including_
intennittent.&.lrcams), mudflats.
sandOats. and wetlands. the use.
dr.gradation or dCs:truction of which
would affect or could uffcct inlr.rs1:.1_tc or
(S.C. 117.ICiHJII
10-24-80 P11r.l,shcd hv TH£ BUREAU OF NATIONAL A HAIRS. INC. WASHINGTON. 0 C 20037
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forcigll commerce including any ,uch
l j~hich-a.rc· or could be used by
rslatc or fordgn travelers for.
rccrcatlorial or other purposes:
(ii) from-which (ish or ,hcltfish arc or
-
Id be la ken and ,old In l.ntcrslalc or
lgn commerce:
ii) Whkh arc used or could be used
Cor-indUstrlal purposes by. Industries In
l i,talc commerce:
) All Impoundments of waters
rwisc defined as navigable waters
under this paragraph:
fl Tributaries of water, Identified In
p graphs (i)(tH4) of lhls ,eclion.
i uding adjacent wetlands: an~
(6) Wetlands adjacent lo waters
:denlified In paragraphs (i)(I HS) of lhls
,,ion (-Wetland, .. mcaii.1 those areas
'. arc inundated or saturated by
;ur ace or ground water at a frequency
md dur3tion sufficient to suppol"l. and
l under riorffial circums·1aricCs do
; ort. a prevalence of vegetation
ally adapted for life in ,aturatCd
:oil ~onditions. Wetlands generally
"lded play a lakes. 1wamps. marshes.
, • and 1imilar areas 1uch u 1loughs.
· e pothole;. wet meadows. prairie
i\·cr overflows. mud Oats, and natural
I s): Piovided. That waste treatment
ms (other than cooling ponds
ing the criteria or thh: paragraph)
re not waters o( the United State,.
l'Process waste water-means any
· r which. during manufacturing or
r ssing. comes into direct contact
·1 or results from the production or
SC or any raw material lntennediate rlcL finished producL byproducL or
· producL ·
117.2 Abb<cvbtloos.
IDES equals National Pollutant
i arge Elimination System. RQ
I s reportable quantity.
117.l Octermfnatfon of report.able •1llc1. . .
qu<1;ntity_ Hsted with each. · ~
bs ance [n Table 117.l ls det-ennined
l?e the reportable quantity for that
9nce.
bllt t7.J--.Rcpoc1abla Quantiliu or
urdou, Sub,tance•
.Jote.-The Cint number under the column •1-RQ"' i, the n:-portable quanlily in
1 • The numl>cr in parenlhe,cs is the
t equivalent in kilograms. For
1vcnience, lhe t110lc contains• column
g
D
headed -c..icgory"' which 1h11 the code
lclkn "X-. ""A", "O"', ""C"" and "O• utoeiatcd
with reportable quantities or t. 10. 100. 100:J
and SOOO pound, n:1pectlvcly.
""" ... '-"J c.-, ....... --· C 1.000 , .. s-c, ~..., _____ C 1,.000 f•S-CI ,.,_...,_ C 1,boo f•S-CI
~q ..... •,..o• • tO(-C,j.tl ,_,......,, 0 1.000(U7'01 ,_,. 0 s.ooo<uro, • I fQ.<1$-41 -• too (◄S.•I ---0 ._.,. curo, -• t fQ.<ll-tl ,..,._.., • . ,oo 1•s.◄1 ,..,._ C 1.000 t•S<II ~"""' .... 0 s.ooo curo, -• tOO(d,.,tJ --------0 s.ooocuroi ____ ,. ___ .
0 ...,. curo,
~~ .. --0 S.000 CU:7'0t
~~ .. --C ·1.000(•Sotl
~ ~---0 S.000 (2.Z70I ~~---0 S.000 IUTOI
~~ .. --0 s.ooo C2.Z 10I ~Ca,t,o,,\<I .. __ 0 1.000 CU701 .......,..,. ~---0 1.000 (U70I -------C J/.100 ("Soll ~di, _____
0 s.ooo (2.l 7'0t ------0 S.000 CUTOt -"""'"---0 . s.ooo (U7'0I ~~--C 1.000(<IS--4) ,.,..__,.....,,. ___ 0 .s.ooo (U70I
~ ~--C 1,000 C•S--4J
~~-.. _· __ 0 s.ooocuroi ------0 1.000 CU1'0I -------0 S,000 CU70I ~IM1r ... ___ 0 S.000 a.zro, ~ ..:.:::.:r-.. __ 0 S.000 CU101 .................... __ 0 S.000 CU70I ---C 1~(,tS<II
C 1.000 <•S-CI
~ p...tw,i,,;,ldo. C 1.000 ('S--41 ~ ~ ........ ~ .. .._ C ,.ooo .... 5-fl -C t.000 (<1S<II ~~---C 1,000 (•S-CI
~ ~---C I.PX> (<IS--41 ---0 1.0():) (Ul'Ot ----O· l..000 "-'"" ,t,,.-.c:~----0 S.OOOIU1'11 --------0 l.000 "-'"" N'Mften;,,,old,t 0 1.000 CZ.Z70I "'-'<----4e 0 1.000 (U701
e...._q-....a. • 101•.s--c1 --C 1.000 , .. ~, a-o;ce,c;,, 0 1.000 IU70I --C 1.000 c•s-c, -C 1.0001-cs-c, ....,,._ • tOO(d.<IJ
~ ~---0 S.000 cz.zro, ..,,..,....,.,, 0 S,000 (U7q ,e-.,.._,... ... 0 s..coo a.z 70I ..,,,. __ .. 0 1.000 CU10I ......,.,._.. .. • 100 (<1S.-c1 ........... C 1,000 , .. ,...,
""'r.c ..od 0 ,.ooocuro,
~~ .. • 100 (<1S.-c1
~ ~----• 100 (<1S.<1J ~~----• 100(-cS.•I
C.lc:iiufol.-..-.. C 1.000 c•s-c1 c.io,._,_...... C t.OOO(•S--cl
Ca'°""'~ 0 s,ooo (U70, C.ic.-O'WOONM ____ C 1.000 C•S-CJ . c..-.:--cy~ • ,o ,,.s..,
c. ..... C 1.0001,s-,;1
~-..,llor\l, ...
~ f>rooc;NonM ___ • 100 (•~··· c-, • 10 C•.S<II
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FEDERAL REGULATIONS
........ c......, """, --:-i .,.....,,. I IOO(d.<11 c.,..., • . 10 f•.s.-t1 c....-0 1.000 (U:7'01 c.... ... ____
0 lJ)OO(Uro, ,_,_. • I fQ.,tS-CJ
°"""" • 10 <•.s.-c1 ,,__ • 100 f•S.•1 0 .... "-'"" • 1 fQ.d---CI 0-"...,_. ___ C 1.000 (--cs-c1
°""""''°"' C 1.000 1--cs-c1 °""""' .,;, C 1.000 (•S-CI °""""' ...... C 1.000 (•S-CI -C 1.000 (<IS-Cl
eo.-C 1.000 (d,<1J C..-----C 1.000 (◄S--cl """°""""""'----C 1.000 (<IS.-CJ eo-.-• 10 1•.s.i1 c,-, .c 1,000 l•S<II
"'---' I 100 f<IS.-CJ
"-"-I 100 (-CS.<11 C&,,p-f,::ac,to•-• I 100 (--C1.◄1
"-"-• 10(<1.S-CI
Cwp-'c;M"• .. · I 100 (-CS.◄I
C,c,ncolJN .. • 100 (◄S.<1J
C,c,nc ......... • 101<1.S-CI
C,c,nc ......... _,..,<Id_ • .. .100 (<1S.◄1
Q,e,rie:WY• .. ·, 100 ,,s. .. ,
Ct~~---• 10 {<I.S<II ~-C 1.0001◄~1
t.•-OAoid .. 100 , .. s. .. ,
t.4-0E~ • 100 (<1S.◄J oor • I fO.◄S-CI -.. 1 (O..,tS-CJ ~. C t.OOO(<IS-CJ .,.._ C t.000 t•S<II -• I (0.-CS-CJ --• 100 (<IS.<11
()ict,lo,op,op• 0 s.ooo CU7'0I
Ov.io.op,_¢4) 0 S.OOO(U7'0I
Ov,lo,op,¢4) • 0 .... <Uro,
O;.;,1o,op,°""""'~
l.J-0,(:f.io,op,(4)0.: eclcl _ 0 S:,ooo (UTQI
""""""°' • 10 (-C.5-41 ........ • 1 (O.◄S-<IJ
~ C. t.000 c-cs-c1
0w, ... ,1o..➔ C 1.000 C•S-CI -C t.000 C•S-CI -.c t,000 (<IS<II -----C 1,000 (-CS-CJ
C t.000 (<IS-CJ • 'fO.,<IS-CJ
"""" • 100 (-CS.<11
D I •"' i:i:• ~ eoid. C 1.000 (-CS-Cl -• 1 ro.•s-c1 ....... • I fO.•S-CI
['1'Q,bo,,.,d,' C 1.000 (<IS<II
'"""" • 10 (<1.5,IJ ,..,_,._ C t.000 , .. ,..,
C"'tkN d.-ir-i C ,.ooo (<IS-CJ
Er+--~---C 1,000 (4$-41 Elhy"-'"'!' o.:Hond,t ___ 0 1.000 tt.z7'0I [OT 0 S.000 CUl'OI ,--c~o ...... __ C ~-;•.:=::~:--f..-ric'~----~~----c. ,--=-~ C 1,000 (.is--c,
f.,4c~ • 100 (<IS.<11)
F..-ri::Mr•._ C t.OOO {<IS-cl f.,4c ....... C 1.000 (-CS,,11 ,_~...., ... _ C 1.000 (<IS-Cl ,-~ • 100 (d,<11
F-...toull, .. C t.000 (<1S-CI ·--C 1,000 , .. ,...,
FOi""'< ecid 0 S.000 CU7'0I , ......... :cecid 0 S.000 C:UJ'Ot ,,,,.,. C 1.000 (<15-41
C..0,,.,-• I (0.<1S-CJ -• I (O.<IS-CI K<i•~-• I (O.<IS,,11
•~rdo....;:t.io.C.oci 0 S.000(2.lro,
~~K-..1 0 S,000 CU7'0t
ts.c. 111.JI ,,.
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REPORTABLE QUANTITIES S·5◄0
131:2053
"""
rcgululion applies to.qu.anlitics o( ~ "" .. dc~ignatcd aubs~•nccs equal lo or i . .......... c.<....-, -.... __. c......, ........ ,._...., ........... greater lhan the r:cportablc quantities • !~ ·------when discharged lnl-& or upon thC i g;: ---• IO(-t.i-11 ........ ..._... 0 l.001 a..z 1'01 it ............... g IOO(d.'-1 ,_,..._ 0 S..OOOP.ll'CM oav(gablc waters oC lhc Unllcd Stales --t.000 (d-tJ ~ttwO--W C ,.ooo t4S41 adjoining 1hol'Clincs. into or up9n the• ,/
loop op o ..... , .. C 1,0()0 (41-41 ....... .,...,. • 101•.SCI l , 11t:1 ·-,_ C ,.oooc•w conllguou1 u,nc. or beyond thC I, ·-0 lp)O(U:0, --... conl.iguou• %one u provided ln acction F ·--• •~.•~1 .............. 0 ~OOC'a.iroe 3ll(b)(3) or the Act. u~pt to the extent ......... M 0 IJ)OO (J.l1'01 ....,,,...,._,... ___ 0 IJ)OOCl.lPOI /i ...,_ 0 ..... "-'"" ~.t-,4to-.,j., ___ C 1,000 1•s..1 that the owner or opcratoq:an ,how 1:: , ... °"""" 0 l.000 Q.l1'0I
........ _.. ___ • 100 t"S.•I such that discharges arc made: i~
L-.f~-0 ,.ooo (U70! .....,._,.,..M C 1,000 Id-ii 1·:::
l__,~ C 1.000 1.s,,1 ......,_ • ,oocd.•I (a) In compliance with• pcnnit Issued i ;~_
lead io,6,d,i 0 l.000 "-'"" ~~ ... --~-0 1.000 Cl.l'1'01 under the Marine Protection. Research ~~ ... ~.:C-0 &.ooo CU1'01 .' f'i
l....;!Mr• .. 0 lp)O(Utq and Soncluarlcs Act or 197Z (J3 U.S.C. ..
l.....i....,_ 0 1.000C:U1'0I
...__ C IJ100 C•1AJ ;
l....;! ....«•M 0 l.000 '2.Z1'0I
~ow-.. ___ C 1.,000 C•1AJ 1401 ct scq.t. 1:. --• '° f<I.S,.,11 ' , ......... D lp)O(U,0, -C ,.ooo C•1AI (b) In compliance wilh I pproved I:.
l-4"'«'J-0 l.000 Q.ll'CII , r, ......... • 'fQ.•S--1 S.-CK..:I C •.000 l•:l-11 water treatment pl.ant operations as .,
""""'•oc..Jolu-J.i C 1.oootcs--1 u,i,,:.-~ .. C 1.000 (CS.CJ t.•~T ..xi • 1C0 (C5,.4J 1pedfied bf locil or State regulations ..... ..,. • '° t•.s-i1 t.•~T • ,co~5..•I pert;tlnlng to ,are drinking water; I:, M-0 1.000 Cl.l1'0I , .• ~, ........ • ICO(d.,•J u.-.:c:~ D l.000 Cl.l'10I t.•.S-T~ • .,co 1•S.•) (c) Pursuant lo the label directions for -• 100 (•S.•t 1,•.S-TP K>d. _______ • 100 1•5..•I application 0£ a pesticide product
""'-C:a,ccy~ • • eo.•s.t1 1.•.S.-TP aco:ll 91.1.,.. ___ • ,oo 1•S.•1 registered under section 3 or section Z4 ""'-C:a,c ,,.,. ... • '° (•.s-c1 roe ' ' co.•s-c1 u.,o.,r,c......,, .. • 10 c•.s.t1 , ..... ~ . .,,-~·--------:.-• 109c•s.•1 of the feder .. 1 Insecticide. fungicide., ~-=~ ........ ___ • 10 (•.S-Ct T-""¥Pr°""'°"""\c-• 100 c•S.•1 and RodCriticide Act (FIFRA). as ..... °""'_"""· .. • .10 (•.S-CI ,_.__, .. C I.OOOl•S-CI ...... _.. • 1 to.•S•t ,_ C 1.000 C•S-CI amended (7 J}.S.C. 136 et seq.). or M..,,.__....., • 100 (•"S..•J ·~-' I to.•:l-11 pursuant lo the terms and conditions of .....,.__,.,..M ___ 0 l.000 (Z.l1'0I ·-C 1.000 (41'11
......,,..,,.i_..i,.,;g,, • 100 1•s.•1 ,..,.,.....,..,.. C 1.000 (CS41 :.an experimental use permit issued under .........,_ • I (O.CS-CI ,..,.,._ • IOi•.S-C) iection 5 or FIFRA. or pursuant to an ... """"°M C IJX'O (4S.CI ,~ C 1.000 1•s-c1 exemption granled under section 18 of -......... C 1.000 (•S.CI ~~, .. "'loo"' , .. o,&..,,,·,.. ___ C 1,000 l•S.CI ,...._ 0 1.000(2.ll'OI FIFRA: ..... • 10 (C.S.CJ ·-C ·,.ooo (41'11 (d} In compliance with the regulations --0 I.COO (U,O, u,-,.1~ .. 0 S.000 ll.ll"Cll
~K>d • 100 (4S.•I u,-,.1 ......... 0 ,.ooo (Z.Z10) Issued undr.r section 3004 or with pcrmil
H<:t,. .. ~"""--0 1.000 Cl.l'TOI V~,-.o-0. ___ C 1,.000 (•S-CI conditiO!l,S issued pun:uunt to section ·-.. 0 l.000 CU70I v......i,c...,.i ... C 1.000 l•S.CI ,....,. .. ~ C l.000(C5,CJ -~-----C 1.000 c•s..1 300S of the Resource Conservation and ,....,. ........... 0 S.000 '2-Zrot y....,...... (t,lo,.,,. __ .:.__ 0 l.OOO(Z.ZIOI Recovery Act (90 SlaL Z795: (Z U.S.C.
~'"'"-"'• .. 0 · 1.000 '2.Zl'OI ,,._ C 1.000 C•S-CI 6901): ~Kid C 1.000 (•S.-1 ....... C 1,.000 {C1,;IJ --C 1.000 {C1,;IJ l"-c'..:.u C 1.000 (CS.Cl (e} In co,mpliancc with instructions or·
~~ C 1,.000 {•SCI l"-c_,__c,.io,:,c,.. __ . 0 I.COO (Uro, the On-Scene Coordinator pursuant to -C 1.000 <•1'11 l--C bot•"' C 1.000 (•S-CJ -C 1,000 (•S-CI l",c~ 0 1..000 a.z10t 40 CFR 1510 (lhe Nalional Oil and
..... ~ .. d,a C 1,000 1•s-c1 l-c ~w, C 1.000 (4$,,11 Ha.zardous Substaii~s f>ollution Plan) or ·~· • I fO.•s-cJ l'<-0 l.000 U.l'10I
"~"'=-09'-d ___ • 10 C•.S.CI l-c,,_.. • 10(4.S.I 33 CFR lSJ.lO(e) (Pollution by Oil and ,.,_,.. C t,000 ,,s--1 c-c ........ C t,ooo C•S-CJ Haurdous Substance,) or In · .......... D JJ:100 CZ.Zrot lire:.,,.,.. .. C IJ:100 (Cs.ii accordance with applicable r·emoval ""'°"""°'<Kid ____ -0 -l.000 CU1'0f l-c ,..,...o,wt,ta C 1.0001•s.t1 ,.,._,_ • I CQ.41'11 l..-c ,..._ D S.000 U.l'1'01 tegulations as required ~y section
~o~--D S.OOOCU10I lire: ~~~IC-----0 s.0001u101 311(j)(l)(/\t.
~~...,,t'-c,,._ • IOO{d.•J l..-,c~ C 1.0001•$-1)
~ ~ --D l.000 '2.l' 70t l<nC~,o,r 0 l.000 R.l70t (0 In compliance with a permit i.Ssucd
ll'o11a...,.·w,..:i~-• 10 c•.S,.,11 l"..-.c: ..... w-C 1.000 C•S-CI under I 165.7 of Tille 14 of lhc Sia le of
ll'Ol.lt.....-..._.. .. ___ C I.OOO(CS.CI z~,,.•"-·---·---0 s.ooo '2.11'01 California Administrative Code: ll'vc.1...:.-....__. ___ C 1,.000 t•S.CI l~p:,ta1.:....."'"'°"""-0 S.000 '1.l'10I
_,vc.,u.:..., w-.. __ C · · tJXlO (•5-'I l•~ ........ ---·-···-· .• 0 s,,oo '2.170! (g} from • properly functioning inCrf
"ll'OI.I~~ .. ---C IJ:100 (45,q l"~ ....,.M;t,lot;,,.. _:.:.;.;:.. D S.000 (1.l'1'01 gu system when used lo provide inert
~....:.-~---•. IO (4.S-CI ll'Ol.lt. ........ ~...,. ___ C 100:l(•s--1 (117.l table corrected by H FR 58711. gas to lhe cargo tanks of a vessel:
l"O',.a.a.,;._ ~M _ a 100 l•S.•I (h) from • permitted •ource and ere
~QOM--. • t<11•.:l-11 ! October 11. 1979; amended by H FR excluded by I 117.lZ of this regulation:
l"top,o,,,<K,d,,. 0 S.000 U.1701 65◄00. November IJ. 19791 Pn:.p,o,-.c.,,,...,.,_or __ ._ D UlOO Cl.11"01 (i) To a POTW and are specifically
~ ... ..,.. 0 l.OOOfUP'OI excluded or n:served in§ 117.lJ: or ,..,, ............ ________ C 1.000 ,.~. Subpart 8-Appficability
0.-0-, C 1.ooot•s--1 (j) In compliance with a p~rmit issued
~---··-·---C 1.000 •• ~. I 117.11 Ccneul applic~bility. under section ◄04(a} of the Cle.Jo Water
~ o•<=• ·--·--·---C 1.ooo,.s.c1
~~ ... ' 1 fO.•S.CI This regulation sels forth a Act or when the discharge's are exem~t
S--.. 'C t.000 ttS-CJ determination of the reportable quantity Crom such requirements by section ◄lH(f}
~ ..,._,,.~,--·-··--C 1.0001•s.c1
$oa...,,,. .. --·-·--C 1.000 ttS,cJ for each substance designated as or ◄O◄(r) or the Act (JJ U.S.C. lJll(o). (0.
s.r-.-"<"'-~• .. '• C 1,00(l t•~I h.Jzardous in 40 CFR P;.irt 116. The (r)).
II-9 IS«. 111.1 Hill
1·21-81
1 J 1: 2054
§ 111.12 Appllc.1blllly to dl,charoc• rrom
f.aclUtlc• wllh NPO€S ~rmlb .. I (a) This regulation docs not apply lo:
(1) Discharges In compliance with a
permit under ,ection ◄OZ or thrs Act:
(ZJ Discharges resulting from . I circumslance1 Identified. reviewed and
made a part or the public record with
respect to a permit Issued or modified
under ,ectfon ◄OZ or lhfs Act. and
I 1ubfecl to a condition In such permit;
{3) ConlfnuouSor anticipated
Intermittent discharges Crom • point
source. identified In ■ permit pr permit
I application under ,ection 40Z or this Act.
which arc caused by events occurrinc
within the scope or the rclCvant
operating or treatment S}"Slcms; or
I · (l,J /\ discharge Is .. ,n compliance "-ilh
a permit issued under ,ecHon 402 or this
/\cl-i( the pcrmil conl.Jins an efnuent
limilalion !1-peciUcally .applicable to lhe
substapcc discharged or an cfnucnt· I Jimilation avplicablc to another waste
parameler which has been ,pccifically
identified in the permit us intended to
limit such 1.ubstance. and the discharge I is in COfr.pliance with the efnucnt
limit.Jtion. ·
{c) A discharge results -Crom
circumstances identified. rc\iewc:d and
I made a parl of lhe public record "'-'ilh
respect to a permit issued or modified
under ,ection ◄02 or the Act. and subject
to e condition in such permit." whether
l or not the discharge is in compliance
with the permit. w~ere:
(1) The permit application, the p(!rmit.
or ano'thcr portion o( the public record
f ontains documents that specificaily
denlify:
(i) The substance and the amounl o(
lhe subslance: and -
(ii) The origin and source of lhe l ubsf::,nce: and
• (iii) The lrealmenl which is to be
provided for th~ discharge either by;
(A) An on•sile tre.>tmenl syslem
'
cp.Jrale from any treatment S}'.stem·
eating the pcrmillee·, normal
ischarge: or
(OJ A lreJlmenl system dc'signed to
'
eat the pcrmiltee·s normal discharge
nd which is additionally capable or
eating the identified amount or the
identified substJnce: or · l(CJ Any combination of the above;
{~I llie permit contains a requirement
thal the substance and amounts orthc
lbslancc. ,,s identified in
g
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I 117.IZ{c}(l}(i} and I 117.12(c}(ll(ii} be
treated punuant lei I 117.12(c)(l}(iii} in
the event or an on-sile release: and
(J} The lrcatmenl lo be ·provided ls In
place.
(d) A discharge Is a .. continuous or
anticipated inlenniUenl discharge Crom
• point source. identified In a permil ~r
permit application urider ,cction 402 of
this Act. ■nd caused by events occurring
wlth(n the scope o( the relevant
operating or lrcalmenl ryslems."
whether or not the discharge i, tn
compliance with the permit. Ir:
(1) The haurdous substance is
discharged rrom a point source for
which a valid permit exists or for which
•"permit application has been sutimiHed:
and
(117.12<dl!II corrected by H f'R
58910. October 12. 19791
(ZI Th~ discharge or the hazardous
aubstancc results from:
(i) The contarriin:ition or nonco~tr.;cl
cooling waler or storm water. provided
that ~uch cooling waler or storm waler
is not contaminated by an on-site spill or
a hazardous substance: or
(ii) A continuous or anticipated
Intermittent discharge or process waste
W4'(er. and the discharge orig:nates.
within the manUfacluring or treatment
system~ or
(iii) An upset or failure of a treatment
,y,tcm or of a process producing a
continuous or anticipa led intermittent
discharge where the upset or failure
results from a control problem. an
operator error. a system failure or
m~lfonction. an eq'llipment or ,ystem
startup or shutdown. an equipment
w,1sh. or a production schedule change.
provided that such upset or failure is not
caused by an on-site spill or a haz:ardou~
subslancc.
f 117.fl Appr.cabitlty lo disch.argu from
pub_!kfy owned trutmcnt worts and lheH"
users.
(a) (Reserved(. with lhe exception. of
I 117.lJ(b} below.
(b) These regul:i.tions apply lo all
discharges or reportable quantities to a
rGTW. where 1hc: discharge originates
from a mobile source, except where such
source has contracted with. or otherwise
received written permission-from the
owners or operators of lhe POTW to
dis<.:har~c ihat qu:mtily. and the moLile
II-10 f ...... O ..... ,c' .. , RoC'pO•l,r,
FEDERAL REGULATIONS
source can show that prior lo acccptjng
thC ,ubstancc from an Industrial
discharger. the substance had been
trcatCd-to comply with any eCClu~nt
limltalion under aections 301. 30Z or' 300
(!C pretreatment il~n"dard under 1ecUon
J07 applic.ible lo that facility.
I t 17.14 OcmonatnUon pc-ofecta.
Notwithstanding any other provision
or this p.:u1 .. the Administrator ot the
En,·ironmental Protection Agency may.
on ■ case-by-cue ba_sis. allow·thc
disdaarge of designaled har.ardous
1ul,stances In ·connection with research
or demonstration projects rel:ating to the
prevention. control or abatement o(
haz:ardous substance pollutiOn .. The
Administrator will allow such a
discharge only where he determines that
the expected environmental benefit from
such a discharge Will outweigh the
potcntictl hazard associated with lhe
discharge.
Subpart C-Notlcc of Discharge of a
Reportable Quantity
f 117-21 Notice.
Any person in -:har:;c of a vessel or an
onshore or an offshore facility ,hall, as
soon as he has knowledge of any
discharge ·or a designated haurdous
substance from such vessel or faciH!y in
quantities equal lo or exceeding in any
24-hour period the reportable quantily
dctenn.ined by this Part. immediately
:1otify the appropriate agency of the-
United Stales Government of such
dischari:e. Notice ~hall be given in
accordance with such procedures as the
Secret,1ry or Transportation h.:i.s set forth
in Jl CfR tS.i.203. This provision applies
to all discharges not spccificall)~ .
e.'(cluded or reserved by another section
of thcSe regulations.
I 117-22 PeMICles...
(:,) AnY person in charge of a vessel or
an onshore or offshore facilily who fails
to notify the Uniled States Government
or a prohibited discharge pursuant to
I 117.21 (except in lhe case or a
discharge beyond the contiguoul'o r.one.
where the person in charge or a vessel is
not otherwise subject lo the jurisdiction
or the Unilcd State,:) sh:.11 be subject to
a rinc or not more than S10.()("I() or
imprisonment for nol more than one
year. or both. pursuant lo scclion
JI l(bl(SJ.
!Sec. 117.22bl/
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REPORTABLE QUANTITIES
(Lil The owner. operator or person in
charge or a veucl or an onshore or
offshore facJHiy from which h
discharged a haurdous 1ubstance
de signaled In ,o CfR Part 116 In a
quantlty equal lo or exceeding In any 24-
hour period. the reportable quantity
established In 1h11 Part (except-In the
case o( a discharge beyond the . .
contiguous z:one. where the penon In
cha·rge of• veuel Is not otherwise
1ubfect lo lhe fur!,dlc!lon of the United
States). ,hall be assessed• civil penalty
o( up lo ss,o:;io per v(olatton under
«:<:liori 311(b)(6)(A). AllemaUvely. upon
• determinatlon by the Administrator. a
civil action will be commenced under ·
1eclion 311(b)(6)(D) lo lmpo·se a penally
not to exceed $SO,()()) unless ,uch
discharge Is the resull of willful
negligence or willful miscOnduct within
the privily and knowle~ge of the owner.
operator, or person ~n charge. in which
case the penalty shall not exceed
S250.000.
Nole:: The Admlnalrator will take Into
~ccount the gravity o(the oITenac and lhe
,tandar-d or care·manl(Cal by the owner.
operator. or penon In charge ln determlntng
wbclhcr a dvll action will be commenced
under 1ectfon 311(b)(6J(8). The gravity or the
oITen,e wtll be lntcrpr-cted to Include the ,lu
or the discharge, the degree o( danger or.hunt
lo tf\e pu~lle health. urcty. or lhe
environment, Including con,ldcrallon or
toiddty, degradabllity, •nd dl,~enal
characterhtlc.a or the ,ub,tanc.c. prev1ou,
,plll hhlory, and pr-cvfou, violation or •ny
,plll prevention regulaUona. Particular
c:mphula wm be placed on lhe •tandud oC
cue and the extent of mitigation eITort•
manUcll by the owner;opeulor. or·penon·ln
charge.
ft 17.23 U~blllllcs for removal
Iri any case where a substance
designated as haz:ardou~ in 40 CFR Part
II-11
~66
131 :zoss
116 ls discharged Croft!, any _ves,el or
onshor~ or oITsh'"orc facility ln a quantity
equal to or exceeding the reportable
quanlily ~elennlned by.this Part. the
owner. operator or person ln charge w[tl
be liable. pursuant lo 1ecllon1 JU (f)
and (g) of the Act. lo the United Slate, ·
Govem"mcnt for the actual costs
Incurred In the removal of such•
1ubstancc.. subfect only to the defense·,
and monetary lilllltationi enumerated In
sections 311 (f) and (g) of !he Act.
The Admtnfstrator may act lo mitigate
the damage to I.he public health or
wClfare caused bY' a discharge and the
cost of such mitigation ,hall be
considered • cost Incurred under s.ection
llt(c) for the removal of that substance
~y the United States CovcmmenL
(~c. 117.231
9-28-79 Published hv THE BUREAU OF NATIONAL AFFAIRS. INC WASHINGTON. 0 C 20037
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APPENDIX C
Internal Spill Report Forms
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Cristex Corporation
Oxford, North Carolina
Spill Report
Page 1 of 4
Within 24 hours after any spill has occurred, this spill report must be
completed by the area supervisor or emergency coordinator and delivered-to
the Spill Control Committee chairman.
1. How spill was detected:
Date: Time:
2. Personnel notified:
Date: Time:
3. Outside Agencies/Authorities notified:
Date: Time:
4, Material involved:
Quantity: _____________________________ _
Type of spill:
5. Area of spill and drains affected:
\
Spill Report
Page 2 of 4
6. Equipment involved, type of equipment failure:
?. Normal operating procedures (note any procedral violations):
8. Labeled diagram of what happened (if helpful in describing spill):
'
9. Actions taken and materials used to contain and clean-up spill:
10. Disposal of clean-up materials:
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Spill Report
Page 3 of 4
11, Results of sampling or testing:
12, Names of operators involved, their training and proficiency:
13. Actions taken to prevent recurrence:
Signed:
Area Supervisor
Emergency Coordinator
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I Spill Report
Page 4 of 4
I 14. Spill Control Committee Recommendations
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Include tasks (Accidental-Discharge Prevention Plan amendments,
additional training, equipment modification, containment structures, etc.)
required to prohibit reaccurance of the spill event. Assign an individual(s)
responsible for completing each task, and attach a timetable for task
completion.
Task:
Responsibility: Completion Date:
Task:
Responsibility: Completion Date:
Task:
Responsibility: Completion Date:
APPENDIX D
' Weekly Spill Control Inspection Checklist
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TABLE l
WEEKLY SPILL CONTROL INSPECTION OIECKLJST
Cristex Corporation
Oxford, North Carolina
Month ,19 -------
ITEM SAMPLE WEEK l WEEK 2
FUEL OIL CONTAINMENT AREA
Stains on walls? none
Rainwater accumulation ( in) 0
Rainwater drau, valve closed? yes
Fuel oil in ar-ea? r'lOVl e
FUEL OIL TANKS
Corrosion f'lo,,e
fi 11 lines capped? ~ es
fUEL OIL PIPING (including recirculation)
Leaks norie
Corros1or. none
DRUM STORAGE AR£A(sl
Vents. bunqs. scab secui-e? yes
Liquic! -:>r dye •Jn floor'? nor1e
Dents or cracks? none
OIL/WATER SEPARATOR
Discharge water clean? ':J es
Oil dCCumulat ion ( in) 3
PRE'TREATM.ENT LAGOON
Aer.itors ope rat inq? Y e.s
m1,11mum Oil on surface? SE cor,,e,
r-eco,,...cl.. D.>U.' last sample collected. dote
I nsr>c-ctor 'S Jniti.ils/Date EDI /Jo..'/
Comment,;:
WECK 3 WEEK 4 WEEK 5
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, .... SECT<ION 10.,, .!NDUSTJUALl SEWER CONNECT JON APPLICATION
-----------------·--------· ----·-------
To the City of Oxford:
The undersigned being the representative
at Industry Drive, Oxford, N. C.
RECEIVED
FEB 03 1997
SUPERFUND SECTION
of the ,property located
does hereby request a pennit to· cont_i_n_u_e _______ an industrial sev1er
I connection serving _c_r_i_s_te_x_c_o_r_p_. _______________ _
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which company is engaged in SIC 2256
at said location.
1.
2.
·3.
A plan to the property showing accurately all sewers and drains now
existing is attached hereunto as Exhibit "A".
Plans and specifications covering any work proposed to be perfonned under
this permit is attached hereunto as Exhibit· "B".
A complete schedule of all process waters and industrial wastes produced
or expected to be produced at said property, including a description of
the character of each waste, the daily volume and maximum rates of
discharge, representative analyses, and compliance with any applicable
Pretreatment Standard or Requirements, is attached hereunto as Exhibit
11c11.
4. The name and address of the person or firm who will perform the work
covered by this permit is t• .. 1-11 -8 v· d -1r. ,, 1 . 1am ruce ice Presi ent of MFG
Cristex Corp. · Industry Drive; Oxford_, N. C. 27565
In consideration of the granting of this permit the undersigned agrees:
1. To furnish any additional infonnation relating to the installation
or use of the industrial sewer for which this pennit is sought as may
be requested by the ·city.
2. To accept and abide by all provisions of Ordinance No. 83-8-1 of the
City of Oxford, and of all other pertinent Ordinances or regulations
that may be adopted in the future.
-22-
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To operate and maintain any waste pretreatment facilities, as may be
required as a condition of the acceptance into the wastewater treatment
system of the industrial wastes involved, in an efficient manner at all
times, and at no expense to the City.
4. To cooperate at all times with the City and his representatives in their
inspecting, sampling, and study of the industrial wastes, and any facilities
provided for pretreatment.
5. To notify the City immediately in the event of any accident, or other
occurrence that occasions contribution to the wastewater treatment system
of any wastewater or substances prohibited or not covered by this pennit.
Date: June 6, 1984 -------'---------
Signed ---h-\-lt~!r Ii'----"---'----~, ,r--+-,&~// 'v\_~,
$ so.oo Inspection Feed Paid
Application approved and pennit granted:
Date: ___________ _ Signed
-23-
(po
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INDUSTRIAL USER PRETREATMENT PROGRAM (40 CFR 403)
Initial 180 Day Facility Report 403.12(b)
(Reporting Frequency -180 Days After the
Effective Dace of the Federal Pretreatment Standard)
IDENTIFICATION
NUMBER
IUTION: Do.!!£.£_ attempt to complete this form before reading instructions!
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Company Name: CRTSTEX CORP
Mailing Address: 261 MADISON AVE
Facility Name:_~c~a~r~s~r~EAx ..... c~a~R~P--------
Facility Address: INDIISIRY DRIVE
NEW YQ BK NEW YORK lQQ J 6 OXFORD NORTH CAROTINh 27565
Phone Number: ( 212) 697-9090 Phone Number: ( 919 l 693 6) 41
Number of Employees: __ 1~9~8.i_ ___ _ Number of Shifts: ---'-----
Environmental Control Permits Held for this Facility: ________________ _
1/2097-RZ stipulation 296.000 :.;a)s pf foe) oil
Process.Description:
Nature of Oneration !Production Race' Subcate~orv I SIC Code
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KnittinQ. Dvein<>. & Finishino of.,.._; __ ... I s.,1 R01 1 ,.._ ' I .... ..: .._ -. . -

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Chemicals Utili:r:ed '-----'S.WWw=.bm-i;.... ______________________ _
Regulated Process Flows
Knit, Fabric, Finishing
SIC 2256
Nou-regulatad Process nova
Boiler Blowdowu
Cooling Water Flow
Sanitary Waste Flow
Average Mex1imm Cont1lluous/Batch
Discharge
260,000 300,000 ...b.==-----
75 gpd 75 gpd
1000 gpd 1550 gpd
Total Plant Flow 261,075 301. 625
l!Pd gpd
Wascevatcr Flows
(gallons/ day)
Basis of Measurement
Estimated G P D
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ZO!\JE FAsT GWE e-x. co~ ... _ _
CHET"lCF\1.-l\lAl"11< ... CHE!Y\\CJ\1.-FAl"HL';I fLUOR.ESCEruT
AKYLARYL ETHER __ WH 1 rENll\lb A<:,E !Jr .
i/fi'or;_fifJ!i"Js _____ t:ltEJtil<. Af£.\5TAJ\)T .
FA.TI'f f\fl')INE .... __ D'fE"~ A!:61!:>TAIIIT. R\.)(:)'LAR.'11. Dlifl.lVATII/ES~E:f'llUL',,lfJER$ '0'{£: CARRIER. ~lJLFON PITEt:, PI\ENouc:
COl\lbENSF\TE'" f 1,XIN(:, AG.EN,
MNTHEl-lE" __ . .. -----~CJt:> .. RE.t) __ S2. ...
l:::>ISAZO _ _ __ .. F\C.\D HQ:._ JIL\
LlZ.AR\l\lE FA5T ~~-190"70 t-1 RSE" ~RILLIANT
Pl F&NEIJ
DLSAZC> __ _ _ ........ ACI~ SUJE II?,
kit:) .BLUE' .25'
f\l'Jlti R,l>.Q,UIOl\lONE' N.RAS,PER5E ORJ;ISE SLOE 'i<:r
N IL 'fEW.OW 6WN l\l II.. £1RIU. IAl'l)T
t:i\'S. PE'R&!: l?.Ll>E' 7
.DISPE~E Y~LLDW "t'2..
'LA\/lnl.E" __ 8G.-FF __ ... J:::,1!:>F'ERSE '/f:J,J..DW g-2.
f\J~IL RED FIS ... !:>!SPERSE .REb 117
UTRI\Sll . .!.CARL£LH~F J..IQ 55% _:= ____ .. _________ D~PERSE-8E.t::>_13S"
:~_~,:u::r-G2E.:;-;=~_-:l-l-: -=-____ D\5f:ER::.E __ B._E:t::,_ '13 ~l .,.., "' ex,;,, "' _____ DISPE.f.:SE_.RE:~325 JTRRSll... Rl.)l,\nlE H -BRS
~f--~~~J1!T ------=-------~l$PEF$: _REb 319 . _
_ . lL~RL________ _ _ _ANTHRAG!VIT\10~.---~PERSE B\.\YE _5<,,
~~--REt>..HCO ... ------··---·---____ _ACJb_REl::> ____ _
INl}N_Bl-J'w::K el:,C./~tt:>81-J>CK .. ==--_. ________________ ....... _
~~~~F. -

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• -~-=~•-=-=• ~ -_·:=·~ -:~:: ~~
~I.LOW.. l¼~~r_~r _________ -----···----Ac.11> YE~w 1-\<\
J.Aln!RENE_ORANE,ESLF ___ CIAZO ______ . ..AC.lt::..O~E: 1\1.._
1..JfrnR.EnlE_fllllK.8\.RF ________ AC\!::) __ fsE'b ____ _
____ ,..._ CID .. RE'b _
l½REM: .. .RUCltllt;_SBLf __ D~. _______ AC.It:> RE~_~':'f\(.s")
. l¼RENE 8UlE_GL.f-_ _::-= _ _ _ ____ J:..C.lt::> B\.OE"' __
~E BLOt I.bbl.~ . . .. ACID 8\.\)£: JU;NEi BR U. IJWT .2.F..FF. . ______ . __ . Ac1t:, G\.UE:
H RE1U E: t-lAIIY LfW<:. M; i,J -AC It:> l3 \.\) E'
ITE "1E'ilDi.J.!¼-. ·--Ci;=;-Z.O _ .. ACl'D'tE.L.LOW L\O
~--G-. _ CSENt-m~e eJISEb) .. AC.It) _RED ~5
:tni.r,i::-SCARLET B.. _____ _ _ AC.It> REl:> 11'·\
TE l"'IIIRCC(\) LS NE'l,J
-.~..,.~ ....... 1 .......... ---···-~ -
&tJPf'LlER.
CRD'nPTT)/1) .'1:-'KNOWL~ (C~P.
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\Q\JfLAlllf!IOf\lll'I (d9,<J% NH.::. _________________ _
.14t::,CAu;1~ S6M S01, _ _ ____ .
~llRlC_Aclt:::> ____________ . ____ . _
'. t:ilc ACltL ___ . . ____ __ ...
Al\l)fl'\ Ctll-{)RltlE'. --------·------· ;F\Ll SOPSR
C HEl'"IICA\.. FAf"'\IL'/ S.1.JPPIJ6~
klOR11\ _C\IEJ"l)IC.AL-.
_ .WORT!+ CHE:.frllCJlU::,
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E./\ls .Rl.lST_ FRES:_ -·--soo1or•fCARl301\.lATI:.,l'll\iH'it:>R.0::6 ... CFIRGO/\JIC.Ac•t:. t:>)Wtlll-'1"1 .!.AL"! ;o ~ _ASH __ ( r.q ~ c 0,3 )..(_n)a. ::2 O) J!"« ;i ~,01j) J(['J" C. 1'2:)j.Fe J "
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/IRTE'X .. Rt:::>.. _____ __ _ ___ _ " -A.AR._EJr1t,1 IC.... _ Aflh lf"IO!IJ'-/ ruT~hll"l .VIRTAATE' ALJPl\RTIC. l\c\b SFll..1 PORl"llll..A KOOc..,c.~,C.H0HJ COO(~ 1/2. H::2O
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: A9'\ffiL __ J.J{l L ____ _
~1~A1e__l)LL _____ _ . ----·-·--·· -----·------·--·----------
)AlnnL.'Ja.LDuJ.%-:c______ _ __________ -~--~--__ __ --: ::~~~~-:=:::_=-B~F_Wya~-ci~tf~
'AJ..ANJh_&.~iwr_Su,1;_ ~F-___ _ _______ . _
A~IL-2Mwl\l ,3 REL,_J..t&vlt::. --· . -----. ---·
'_A LFWIJ.._81)8\NE _fl_ ______ _
Al/VIL ___ SUJE__R., _____________ _
'3~Af\J_ f,we_C::,e_trfE:
:-.. AN -~1-A:t<;:_l.B_O-(E'_:i?Af.n: __
':A:jfDl\)E.J'.AST_,SGl\Rt,.IT_&~!ef___l:>~_u~--
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Thiox.
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A~ISILBl..UE_6SR (D!SPE£SE ~Ll)E3) .
FCjOl\l Ill AVY S.-.:2~ ( DI.Sf'EFSE _,8UJE 'l"!J
0ol,1UJ'8.LOLJSE:£,CW(.DISPER\:,E ~E/.1.D(V'-\:i:J __ _
0~-~11.WA/\Jl DRAN':,~ E-RL(DISPERS".: CAAIIX'::E :ls-J
J'i!l:A!U_f\lA\)'f 8LlJE_f\l~ U,C1t::,(3.LJ.)'E 113J
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u'l~_'fEUl)wN-:-SC:r_L(A::1b'H:'i-l.-OWl'::l'lJ __ ··-··· _.
0 N_e..RILLIAiVT:.REl::.S::RC:,L(DIS~~ RE!:0 _. __ ..
'OljN_SRILLIMlT_R£_bS~R6L _LJQv1t:£PLSPE~E RE°t:0
1Rls11 .• Sc:ARLIT GP(P~PER:,E R~~ 1':) ~-◊r ~aer~~-~~~ ~+-~~~~ RE~7q .
--• _, ______ .. _____ ----·•·-------· ----· .. .. . .... .
t:d!L~R._c_liEQJICALS,, · ---·---·-· ·-·--.. -_.
E.llf-EC.--'J_O_'..:,-=_h{Q,$J~HAIE DISF:ERSl'HVT ____ . . _ .
E rlr:Ec..__'7J_~ _ ___::__Al))J lEOArn_ ___ l)_1s F.'= REA.NT. __ Epc.. __ 13_3_:_C)..x.'IG:>EN__&AYS/\)(:,ER. ____ .. ____ .. -· . ·-_. -·
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EN T.EC.~~-'J...:::..CoNt:>E N.SATE'_TREAT!'DENT
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I J
II
61 Nature and Concentration rif Pollutants
Rlulated Process Line
Pollutant/ TSS COD BOD Zn Cu Cr
Units mall ma/ l mo/ mr./ l --/ 1 /1
Pretreatment -
Standard 1000 2500 1000 3 . 4 2
I Maxicium 300 750 300 .16 .22 . 24
I Average 644 141 . 14 .e::n n <n n,
Rtulated Process Line
Pollutant/
Units
Pretreatment
Standard
I Maximum
I
Average
Pollutant/
Tulated Process Line Units
Pretreatment
Standard
I Maximum
Average
I ·Pollutant/
rined 'Waste Stream Units
Pretreatment
Standard
I MAC
AAC --, AMMC
AMAC
I·
Method of· Sample Collection =-~=.b---------------------------
• ·cook. samples, what time and
Analytical work performed by: __ _,G~r~a~i~·u~g~e~r.._T~a~bw.a~r~a~t~a~r~i~e~s~,_.r~n~s~g~r~p~ ...... -------------
1 '-• ■ampling ■nd W. Paul Brafford
analysis performed in accordance with 40 CFR Part 136 m Yes D No, I not, vhy not? ____________________________________ _
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rm
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Grainger
-1,aboratories
!Incorporated
Analytical and
rnsulting Chemists
sJ Commercial Avenue
Raleigh. NC 27612 I [phone]
1040 Greenfield Street
Wilmlngton. NC 28402 1-[phone]
I
I Analyt!cal
Laboratory
Environment Analysis I Materials
I tllication ot Unknowns
AgTicultural Products
I
I
Fuels
Textiles
Hazardous Waste
GC/MS
ICP Metals
Priortty Pollutanls
Consullal1on
Metallurgical Services
I Pollution Abatement
Process Development
Quality Control
Methods Development
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Special Investigation
Cert:Ul=tions
SDWA
NPDES
USDA
USEPA
April 30, 1984
84-10454
Cri stex Company
Industry Ori ve
Oxford, NC 27565
Attention: Mr. Page Hughes
Subject: Analysis of Sample Received 4/4/84
· Sample Identification: Purchase Order No. 1164
1. Lagoon Sample
pH
Chemical Oxygen Demand, mg/1
Biological Oxygen Demand, mg/1
Oil & Grease, mg/1
Sulphate, total as so4, mg/1
RESULTS
Residual Chlorine, total as Cl 2, mg/1
Phenol, total as c6H50H, mg/1
Copper, total as Cu, mg/1
Zinc, total as Zn, mg/1
Chromium, total as Cr, mg/1
Hexavalent Chromium, total as Cr+6 , mg/1
Cadmium, total as Cd, mg/1
Nickel, total as Ni, mg/1
Barium, total as Ba, mg/1
Lead, total as Pb, mg/1
Manganese, total as Mn, mg/1
Silver, total as Ag, mg/1
W-~~-{'.)~
W. Paul Brafford
General Laboratory Manager
WPB/ss
cc: Bi 11 Bruce
1. 9
644-
141_
46.2
81
<0.02
0.24
<0.05
0.14
<0.05
<0.05
<0.05
<0.05
<0.05
<0.05
0.04
<0.05
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Bri'efly describe wastewater treatment system (provide diagram in attachment):
Does your
Yea[i]
See Attachment II 1
facility have a Spill Prevention Controls and Countermeasure (SPCC) plan?
NoLJ
Briefly describe disposal of hazardous waste (chemical byproducts) to include pre-
treatment sludges:
WiJ l coo tact qpaJ ifigQ pli'rS9RB 1=e 8:iopose ef ;.a"ec as needed,
Describe location of sampling manhole: ___ ~o~n:_.:e~f~f~l~u=n~t=-o~f=-=l=a~g=o=o=n'--------------
Describe location of entry of process waste streams to sanitary sewers: ______ _
At an existing manhole on industrial sewer line adjacent to r..1ilrr;;rad
See Attachment # 2
CERTIFIED STATEMENT
Pretreatment standard& are [iJ are· not CJ being met on a consistent basis.
Additional operation and maintenance under consideration for compliance is as
follova.
I Additional pretreatipant under coc■ideratioc to meet at■ndarda ia as follows:
None
n
0
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ATTACHMENT -# I /
\
7o. lJ~ ~
D. Normal Process Vater Flows
. Vastevaters from the various dying and' finishing processes within the
plant flow by vay of process sever to the pretreatment lagoon. The lagoon
has s surface area or spprox~mately 1/2 acre and a volume at 5 foot depth
of 0.8 million gallons. The lagoon, when aerators are installed, will
function as an aerated treatment lagoqn with approximately 3 days average
.
-
hydraulic retention time. The pretreatment system will function as both an
organic removal and waste equalization system. The effluent piping is
designed for subsurface dravof! to prohibit floating oils from entering the
city sever system. The effluent end of the lagoon will remain unmixed
prohibiting the discharge of solid material which may cause obstruction in
the sever system.
~~ CUUL JJY\., ~
-
1-
2
UJ ;:::
:r:
~ ~
<(
- --
,'",.,
,:->-
. ~\): ·:_: '\t
.·i :· .:-;
:--!--,'}
··' . . -:·
•' C.~ • •
. .. )~~-. '.· ,(';ii,
--
uel
To llighway 15
--B!!!I l!S!i:il iiiii ---
Pretre<!!Ullent
Lagoon
rigure 11 Site Plan
Discharge to
PON
Cristex Corporation
Oxford, North Carolina
-- -
ul.If pr_e_creatmenc
comp l:iance:
standards are not being met, complete the follo"1ing schedule of
I
Increment
la.
(1) of Progress
N/A
d.
I
e. -----------------------1
Scheduled
Commencement
Date
(1 .. No increment of progress shall exceed· nine (9) tmJnths.
(211Final. c0111pletion date should not be later than c01Dpliance date.
Scheduled(2)
Cotll1lletion
Date
JI .. I certify under penalty of law that I have personally ex.a.mined, and am familiar with,
t information in this application and all· attachments and that, baaed on my inquiry of
those persona 1-diately ·responsible for obtaining the information contained in the ap-
plllJ:atiou, I believe that the informatiou. ia t~, accurate, and complete. I am aware-
cbl); there are sipificant penalties ·for subm:itting false information, including the
possibility of fine and impriaonn.nt. (See 6/26/78 Federal Register, Section 403.12(k)
fol information on signatory.,
1 .Mr, Wi~am Bruc.e .... Vice President of MFG
Official Title
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CnY OF OXFORD. NoRTH CAROLINA 27565
120 WILLIAMSBORO STREET. P.O. BOX 506 -<919> 693-2195
OFFICE OF THE
CITY MANAGER
Mr. William ErtlC0
Vien: Pt£~ . .:::ic!r:.nt 01 Manut:acturing
Cristax Corporatior~
l ridt.H¼ try D.r i VE:
(lxfurd, ,.:. C. 27:,6$
Dur ins & r-'.:-!cf1.nt r-evi<~.w.' of ::our i.ndn:::lri.al we.19ti::'VJC.t.er pen1ti t.
\•12 noticed tr.at a lir.~it of H~i,nc:; :?D1 .. f~(:r doy h'5~~ b{:-:.\~n r..i:.::t:A:tin<:r-
ly usod. WZ?. a1•f:-!. her•~b~• ~v11t?riOin~: t;"'11.~ Cri ;~t1~:~: y.1ir,.r:r:Jt -::o r.~crt~
-a~e~uately re~.!.ect your actual flow to a D~rmit.t~ci discnarg0 0f
45,0,DOf; 9ei_l/-:3.:1y.
Ct:rt·,:::n.t:i;: t,~ ai'::: t,t:'.!.;:..:-c::..;.l.:::-:\ t.c:, ;,"i-:1;1.it.:~~1:i:'."1-::_~ Cri!:·.:,:-.;:~ :~~er r.h,;;•
f. o 11 ::,.-.,; i. n.,::, ::::;~ r: 2.L;:~~ \:;:i: r ~; :
DVi:-, } d~y
PhC3£)horc~i
·• ~ p··
Zinc
t:c:pi;:.,~f"
tot.al ~:~:rc~ium
r:exav~lent Chromium
I'1·ivttl~::nt. Ci'..r.c1:,i'J1~:
Sil!CAI your ~fl:l.u-=Jnt '.°i<:!,~; be,:-:n in c...:.q-:,p.1.ian~e -...iitl·i Ell of tn<:~82:
p.:..i.t~E~i:ste:~:::, \•,hi! i,.,.:-ill, hc~nc'G(or.:U·:, ~non.itc..?: ::.-:..:: r .. ;'.:.~·., f: ... c.n., ·1•··
and oil arid grease ~n e ~onthly ba~is cn0 r)onitcr ~er ~J.l ct.:
these paramHt~rG once a y~~r.
The (:ity of Oxford's Pr(:tr-c•&t.s;1<:!nt PLoq::,,in watt adopted on
;~.usust 9, i~di3. In f.!)irPe~•,s ::v cnch of t.!.,1:? in~}i,;i;tril:!.& u::-i1i~1 the
City'u !::~'3WC!'a:;1~ sys-terr. w~ ::ave e;.;.to.l:,ll:r.h(±d .Jul:.~ 1, 1~84 n:•:i. the
dat.& for :)<B<Jir.ning of cal.culat.i[11J. CC·St ,..Jn indtji;t1~tal :'i'l.1.rcharq,:6f;:
and mr.:,nitor1r~tJ. Si:ice J 1.,ly 1, 1984 tht~ Ct·istex -?.~fl1Jt:tnt ~1aH b"::·2n
t>elcu the s~~charge thrcst1010 l25(i ppni for 8.0.!'. & -~.S.S.).
Thc-.rt"!:-'ore, thf!'re: is nc :;;nrchr:i rgr~ fer t.hif'. Lu2t ii:-;.c£\1 yc~J·.
Below iD a list of t~1e ~0nitoring char;es tor :t1e y~Rr.
111 2.u~'T'!:-::ary, it. u~ernr~ ':".f·1e11': th~ tH:r.1tlon •~.t~vic~::!£. \\'hic1·, yuu
i:1:t3ller. .Co:-F-l~{!t.r::'.'~1:r~,f'.~'l'.:. l~: yot:r la9':)on are p!~rforri:lr,,J \rt(~ll.
Ye~ a.re to b,::; Ci~nqr~1tnlate..:i ~-C';r thi,:i ;:;ro,;;rf:.~12iv-= "ction.
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Mr. William Bruce
Vice President of Manufacturing
Cristex Corporation
Industry Drive
Oxford, N. C. 27565
Dear William:
NovP.mber 7, 1985
We have been informed by the Division of Environmental Management that we cannot
delete the test for any of the parameters of the pretreatment monitoring program
without their approval. Therefore, we will have to analyze for all paramenters
listed in the pretreatment program until we obtain their approval. This means
we will have .to run the complete analysis on all 14 monitoring events at Cristcx
and bill you for these.
We will continue to ask the Division to reduce the number of test required when D an industry has a good record of industrial wastewater treatment such as Cristex's.
m Your attention to this matter is appreciated.
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J:''f 21A A
JESSE A. SULLINS, JR., P. E.
cc: H.· T. Ragland, Jr.
William Pritchett
123 North Mnldenbuq,:: Ave.
South Hill, V.i. 23970
(804) •l/47-7621
316 East Third S!rt:ct
ChJ.St' Cily, V;i, 2392·1
Survey -[phone]
L;ib · (80'1) J72-'.U9J
CITY OF oxFORa
0 FILE-NO RBGf'ONSB
0 FILE -W/COPY l'!EPl.'1 .
REC'D NOV 8 100'5
0 COPY(IES)TO
0 REROUTETO
0 RESPONSE ON TAPS
I'. 0. Hnx 248-109 Littlejohn 51.
Oxford, Nor1h CJrolin,1 ~75fi.'i•0~-IH
(919) (193-D.l".?
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OFF1CE OF THE
CITY MANAGER
Mr. Reginald Joyce
Plant Manager
February 25, 1986
Oxford Printing & Finishing Industry Drive
Oxford, N.C. 27565
Dear Reggie:
Oxford Printing & Finishing Companies surcharge cal-culations for the fourth quarter of 1985 are shown below:
1. B.O.D. (max.)= 1,037 ppm Flow= 3,890 gal.
pounds B.O.D. = (3.89 MG x .8)(1,037 -250)(8.34) = 20,425.9#
B.O.D. Surcharge =(20,425.0)· ($80/T.lbs)
1,000.0
= $1,634.07
2. T.S.S. (max.) = 540 ppm pounds T.S.S. = (3.89 MG x . 8)(540 -250)(8.34) = 7,526#
T.S.S. Surcharge =(7,256) ($80/T.lbs.)
1,000
= $602.13.
3. Monitoring cost,2 events= 2($250) = $500.00
TOTAL AMOUNT DUE = $2,736.20
Hydro Management, Inc. will be conducting the City of Oxford's Pretreatment Program as of March. This is part of their operational contract with the City. We plan a visit to introduce them.
If you have any questions., please call.
cc: B & B Consultants
Doris Hayes
Sincerely,
,,-:;r--7 ; 9 ,f.' /(._....-
/
H.T. Ragland, Jr.
City Manager
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• ,-.·~~.~ ... ~~-j ••• -_ •
Below a' 11st··o"'
nances during the paSi six . --
1.
2.
3.
4.
Industry Date Parameter(mg/l)
Cristex Corporation
Action taken: a.
b.
C.
Result Limit
11-25 & 26-85 (181) (0.5)
Industry was asked to check chemicals used
Resampled zinc and was back within limits
Wastewater Treatment Plant analysed for zinc
(results were a little high -

2

mg/1)
Burlington 8-8 & 9-85
8-8 & 9-85
Cr 3+ (1.31) (1.00)
Cu (1.97) (0.4)
Action taken: Burlington was asked about cause of high copper.
They resampled and results were satisfactory as
was a subsequent routine analysis. High Chromium
was thought to be analysis error since it did not
recur.
tlax Factor 11-12 & 13-85 P(6.0) ( 5. 0)
Action taken: None (marginal violation)
Oxford Printing &
Finishing Company
10-15 & 16-85 Cu (1.82)
Action taken: Industry has recently installed Pretreatment
facilities and asked to check for sources of
Copper.
H.T. Ragland, Jr.
City Manager
(0.4)
@
----=-------_ -"_=_ --.. ----•--..<:
---' .~~ .. ·~·-.,,· .. ~ ·~-........ ,· ~·-··:,.•:i~.;:.,:~oi:."'J~~':.~li.:'~;1;,,t,."!,fo~i'!i.:-.;,i,•;;.r,'.;;@;~~
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CITY OF OXFORD. NORTH CAROLINA 27565
120 WILLIAMSBORO STREET. P.O. BOX 506 -<9191 693-2195
OFFICE OF THE
CITY MANAGER October 7, 1986
Mr. Sam Moore
Burlingtcn Research,
P. 0. Box 2481
Inc.
Burlington, N. C.
~De,,"'• ~o,e,
27215
Re: Cristex Corp.
';-Jater and Sr~wer
Oxford, N. C.
u
D
Pursuant to one telephone conversation of Cctober 6, l'J&G in
reference to flirnishing water and sewer to the Cris~ex Plant in
xford, the.re is transmitted herev.1i th several Uc-cumc:·nts whic!1 ar€.~
ertinent to water and sewer usage.
Document::: included. are cc-pie.s cf our Sewer !Jsc Ordinancf:,
th~ Pretreatment Ps:ograrr., a copy of the Cristex di.scharqf.?: pE:rn,it
an<J etc.
We contracted out the operation of our wastewater treatmc~nt
plants in February cf this year to Hydro ManagerneI1t ServicGei,
Inc., P. O. Box 1279, Clemmens, !'.J. C. 27012. ~c. C. D. Malone i::;
president of that firm and technical questions on ~ewer use uiay
be directed to him at (919) 766-D?.70.
Due to the fact that Cristex was our largest 1-.ater and sewGr
user, we are anxious to have another similar user to take their
place. Therefore, we do in this instance encourage a relatively
large water and sewer u,-,er to t;ake the plar::e of Cristex.
Please feel. free to call on tis for any assistance that we
can give in connection with a changeover ir1 the Cristex Pla~c to
a new use!'.
One note of caution is that we want to have the op;:;ort.unit.y
of reviewing the proposed wastewater analysis of ,., new user price
to final commitments. We would expect no problems but it is
always best tc have a complete understanding on t.hese matters.
HTR,Jr/ap
Enclosures
Sincerely,
B. T. Ragland, Jr.
City Manager
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I ACTUAL USE AND ACTUAL BILLING
.CRISTE! CRISTEX CRISTE! CITY CITY CITY CITY CITY CITY
I MILLIONS WATER SEWER TOTAL .WATER SEWER TOTAL
MO GALLONS BILLING BILLING BILLING BILLitrn BILL!t/G BILLING
9-86 3,025 2,181 2,74B 4,929 42,911 5.08, 51,600 5.331 94,511 5.221
8-86 10,40B 7,259 9,146 16,405 52,370 13.861 57,433 15.927. 109,803 14. 94l
17-86 14, B96 10,176 12, B22 22,998 54,047 18.831 59,500 21.551 113,547 20.251
6-86 13,964 8,702 7,324 16,026 48,397 17.981 36,244 20. 21l 84,641 18.931
5-86 13,917 8,692 7,301 15,993 45,438 19. 131 34,784 20.991 80,222 19.9\I
14-86 11,959 7,537 6,331 13,868 42,085 17.911 32,018 19.771 74,103 18. 71I
3-86 8,331 5,329 4,477 9,806 38,065 14.00l 28,646 15.631 66,711 14.701
2-86 10,158 6,474 5,438 11,912 43,457 14. 907. 42,483 12.807. 85,940 13.861
11-86 6,510 4,182 3,513 7,695 38,590 10.84l 38,373 9.15I 76,963 10.00l
12-85 4,407 2,897 2,433 5,330 34,480 8.401 26,499 9. 181 60,979 8.741
11-85 9,642 6,155 5,170 II, 325 43,328 14.211 32,569 15.8/I 75,897 14.921
110-85 9,206 5,881 4,940 10,821 41,755 14.081 31,948 15.461 73,703 14.681
------------------------------------------------------------------' ---------------------
12 116,423 75,465 71,643 147,108 524,923 14.381 472,097 15.187. 997,020 14.751
I ACT~AL USAGE WITH THE NEW WATER RATES APPLIED
0 MO "GALLONS NATER SEWER TOTAL
9-86 3,025 2,181 2,748 4,929
8-86 10,408 7,259 9,146 16,405
7-86 14,896 10,177 12,823 23,000 D 6-86 13,964 9,571 12,059 21,630
5-86 13,917 9,540 12,021 21,561
4-86 II, 959 8,267 10,416 18,683
• 3-86 8,331 5,841 7,360 13,201
2-86 10, 15B 7,096 B,941 16,037
!-86 6,510 4,585 5,777 10,,,62 I 12-85 4,407 3,134 3,949 7,083
11-BS 9,642 6,746 B,500 15,246
10-85 9,206 6,445 8,121 14,566
--------I 12 116,423 B0,B42 101,861 182,703
I THIS WORKSHEET DEMONSTRATES THE IMPACT THAT THE CLOSING OF CRISTE!
NILL HAVE ON THE OXFORD WATER WORKS. A SUMMARY IS AS FOLLOWS:
I CRISTE! HAS CONSUMED 14.381 OF THE CITY'S WATER AND WILL
BE BILLED FOR 15.18% OF OUR SEWER CHARGES, FOR A TOTAL .
!NP.ACT ON THE REVEtlUES OF THE NATER SYSTEM OF 14. 75I ON THE OLD RATES.
OF THE NATER AtlO SEWER REVENUES OF THE CITY OF OXFORD.
I THE TOTAL BUD6ETED WATER AND SEWER REVENUES OF THE CITY
ARE $518,000 FOR WATER AND $508 1000 SEWER FOR A TOTAL OF $1 1026,000
TIMES 17.80I, BASED ON THE NEW RATES, WHICH IS CR!STEI SHARE, TOTALING $182,700.
I THIS MEANS IF ANOTHER PLANT DOES tlOT USE THE SAME AMOUNT OF
WATER AND SEWER THAT CRISTEI HAS IN THE PAST THE CITY NILL LOOSE
APROX $15,000. PER NONTH WHICH COULD EQUAL SlB0,000 PER YEAR DN
I THE NEN RATES.
THE' WATER l SEWER AND THE FINANCE CONMITTIE NEEDS TO BE REVIEWING 1'.
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PO}SIBLE AREAS THAT SlB0,000 CAN BE NADE UP FRON.
...
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CITY OF OXFORD. NORTH CAROLINA 27565
1 22 WILLIAMSBORO STREET. P O 80X 1 307 -(9 1 9) 693-2 1 95
OFFICE OF THE
CITY MANAGER
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
Mr. George J. Christensen, Jr.
Cristex
Oxford Division
P,O_ Box 527
Allenwood, NJ 08720
October 9, 1991
Subject: Lagoon Discharge to the City of Oxford's
Sewerage System
Dear Mr. Christensen:
The City is experiencing a great amount of infiltration/inflow to it's sewerage system and has discovered tl1at some of tl1ehnflow is coming from the lagoon at Cristex's former plant. The purpose of this correspondence is to inform you that you should take steps necessary to connect any domestic type (restrooms) to the sewer system because we will eliminate the discha1-ge ft-om the lagoon to our system. We plan to take tl1is action on or after November 1, 1991 whicl1 will be to disconnect the effluent from your lagoon from our manhole in the City of oxford's right-of-way.
Your attention to this matter is appreciated.
,,}~7( -&-(:. T. Ragland,
City Manager
HTR,Jr/dn
cc: Jesse A. Sullins, Jr., City Engineer/
Jimmy crews, Public Works Director
Judy Garrett, DEM
)
.• For~ 3!3 ~,~ ;: ~-1:9 i{!~f i~·~~GP.:~-,"•i,2~-~~~~\(.l;~:', ··. ~~-"'~~~~ ~=T~~N. R:_CEIPT
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P.O. Box 527
Allenwood, NJ ·08720
Subject: Lagoon Discharge to the City of Oxford's
sewerage System
Dear Mr. Christensen:
The City is experiencing a great amount of infiltration/inflow
to it's sewerage system and has discovered that some of the~nflow
is coming from the lagoon at Cristex's former plant. The purpose
of this correspondence is to inform you that you should take steps
necessary to connect any domestic type (restrooms) to the sewer
system because we will eliminate the discharge from the lagoon to
our system. We plan to take this action on or after November 1,
1991 which will be to disconnect the effluent from your lagoon from
our manhole in the City of Oxford's right-of-way.
Your attention to this matter is appreciated.
Ragland
City Manager
HTR,Jr/dn
cc: Jesse A. Sullins, Jr., City Engineer/
Jimmy crews, Public Works Director
Judy Garrett, DEM
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Cristex Corp., P. O. Box 527, Allenwcxxi, NJ
Mr. H. T. Ragland, Jr.
City Manager
City of Oxford
122 Williamsboro St.
Oxford, N. C. 27565
Re: Lagoon Discharge to Oxford Sewage System
Dear Mr. Ragland:
08720-0527
CITY Of OXFOII.O
D I'll.I! -NO RfSl>OHSI
D AD: . w / COPY U>U'
flC:T 31 1991
D COPY(IES) TO
D RUOUTI: TO
0 RESPONSl: ON T AP1
Pursuant to your letter of October 9th, 1991 regarding an
infiltration flow problem with the City of Oxford Sewage
System, we are unaware of any problems associated.with
the waste water discharge from our lagoon to the sewage
system. As you know; the manufacting plant now owned by
Cristex has dTscharged waste water to the system for over
twenty years. In this period of time, we have consistently
complied with City, State and Federal waste water guidelines.
Since receiving your letter of October 9th we have contacted
the North Carolina Department of Environmental Management
and various environmental engineering companies in order
to review this matter.
Because of the totally unexpected. matter of the infiltration
inflow problem with the City of Oxford Sewage System, coupled
with an inadequate reaction time to meet your deadline of
November 1, 1991, we request a extension in order to formally
submit a course of action.
We :shall await your answer of this matter.
Sincerely yours,
may
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
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CITY OF OXFORD, NORTH (:AROLINA 27565
1 22 WILLIAMSBORO STREET. P. 0 BOX 1 307 -(9 1 9) 693-21 95
OFFICE OF THE
CITY MANAGER
Mr. -George J. Christensen, Jr.
President
Cristex Corporation
P.O. Box 527
Allenwood, NJ 08720-0527
Dear Mr. Christensen:
November 4, 1991
The City of oxford is hereby granting your request for an
extension in order that you may prepare plans for a course of
action to remove the lagoon discharge at tl1e Oxford Cristex Plant
from our sewerage system. This extension will be for one month
until December 1, 1991.
we will negotiate the amount of time required for construction
of any approved facilities.
Your attention to this matter is appreciated.
HTR,Jr/dn
cc: Jesse A. Sullins, Jr., P.E.
Jimmy crews
Ragland
Manager
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CITY OF OXFORD. NORTH CAROLINA 27565
1 22 WILLIAMSBORO STREET. P. 0. BOX 1 307 -(91 9) 693-2 1 95
OFFICE OF THE
CITY MANAGER
Mr. C.D. Malone
Hydro Management Services, Inc.
P.O. Box 1279
Clemmons, NC 27012
Dear Mr. Malone:
May 20, 1992
I wanted to call to your attention the laboratory report
submitted by Webb Technical Group, Inc., a copy of which is enclosed,
in order that I might propose a question to you in reference to the
matter of the sewer lagoon at the Cristex Plant on Industry Drive
just outside of the corporate limits of Oxford. For some time now I
have been concerned about what effect the overflow of that lagoon
into the sewer system might have in connection with the Wastewater
Treatment Plant. Please review this report at your earliest
convenience and advise me of your opinion concerning the proper
course of action that the City of Oxford should follow to resolve
this matter. I see this subject lagoon as being a potential
contributor to our overall problem at the Wastewater Treatment Plant.
I do not have the technical judgement that you have on these matters
and I need your advice concerning the indications of this report.
Thanking you for your kind
HTR,Jr/dn
Enclosure
assistance in this matter, I am /.'
SincereJ.y'; .· .·// /17)(,,,,:J/ ,,:''. 1/ ck~vt'o/~
H.T. Ragland, Jr.
City Manager
ge 1 Webb Technical REPORT Work Order i 92-04-333
ceived: 04/09/92
REPORT HYDRO MANAGEMENT SERVICES/
TO ~O~X~F;O~R=D~WW~T=P------,-----
POST OFFICE BOX 1301
. ,. OXFORD,' NC"0 27565
ATTEN MR. JOHN POTEAT
CL+EN_T .. "'H~M"'O_'__,,---'---
OMPANY HYDRO MANAGEMENT
CILITY OXFORD WWTP
SAMPLES _l
SERVICES/
····~"-....... CLEMMONS . NC
:o WW MONITORING
TAKEN CHRISTEX
TRANS PICK-UP, T. KRIZ 2/2
TYPE WASTEWATER
~. 0. #
~OICE under separate cover
SAMPLE IDENTIFICATION
CHRISTEX-9 COMP 4/9/92
. ··. ·. ·~ :··.·.· /;f;~;.-.
AG
Cb
CR cu
HG AA
NI
PB AA
ZN
04/20/9212:12:52
PREPARED Webb Technical Group,
BY 4320 Delta Lake Drive
Raleighi NC 27612
ATTEN.ClientServices
PHONE {919)787-9171
Inc. ~LL CERTFIED BY ,
CONTACT G FLYNT
We are oleased to provide this certified report of analysis.
Samples will be retained for 30 days after report is issued.
Feel free to telephone if further explanation is required.
Refer to the Work Order# in all correspondence.
COPY OF CHAIN OF CUSTODY TO HYDROMGT. FOR PRETREATMENT ONLY.
cc of report to: HYDRO MANAGEMENT/ MS. NADINE BLACKWELL
P. 0. BOX 12 7 9 ,
CLEMMONS NC 27012
TEST CODES and NAMES used on this workorder
SILVER
CADMIUM
CHROMIUM, TOTAL
COPPER "
MERCURY BY COLD VAPOR
NICKEL
LEAD BY AA
ZINC
- --------l!!!!!!I I!!!!! == liiiii iiil - - - -..
age 2 Webb Technical REPORT Work Order# 92-04-333
aceived: 04/09/92 Results by Sample
SAMPLE ID CHRISTEX-9 COMP 4Z9Z92 SAMPLE # 01 FRACTIONS: A
Date & Time Collected ri4/09/92 10:30:00 Category
AG <0.01 CD 0.115 CR 4.40 cu 4.65 HG AA 1.24 NI 0.469
MG/L MG/L MG/L MG/L UG/L MG/L
PB AA 0.954 ZN 29.8
MG/L MG/L
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SMITH HELMS MULl-15S & MOORE
<.:.._ARLOTTC OFFICE:
1-CAILIHG AOORCl.$
ATTORNE'..YS AT LAW
RALEIGH, NORTH CAROLINA
MA/l.1N¢ #,OOIH:ss ~nu::CT .AO()l',CS,i
'.i~CE"'··. -, , :_,, ... ice
,..,..,: :,,,; .-r::,;.;cr.s
PQ;;T c, .. r,<;:t: 60.X 21,:,2;7
ORCLN60()H0, N, C, 4 7 .. ;::Q PO:OT or,1ce BOX 312"'7
CHA.R\.OTTC, N. I:. zoz::11 P0BT orr1cc ■ox ;,p~z !;
.. .-.<.11":l()H, N. C. 21<'111
316 WC&T i;:oc1,noo,i !;TIJ<f".f".T
6HU:cT AD011"C:11!i
ZZ7 NQ#tTM TRYON STACl':T
CMARLOTTt., f'l,C, ZOf:'02
TCLCP0'10Nc'. 70"'-/343-~000
TCLl':COPll:'.R 70i./J.:l••o•<;l7
TCLt)( ~,-, .... oo
Jesse A. Sullins,Jr.
City Engineer
Oxford,North Carolina
Dear Mr. Sullins:
/;ALCIGM, N, C, 27fi0~ 1'
n:u:P><IONI: Vlljl~(;lkl;>.Ol::01
ri:::o.it:CQ.-,,CI'< '119/626-7936
0,TRCCT AOORl:'ii&
6lllll , .. 00
300 NORT!i GRt;UH, ~H•C:r'.T
GRC.C:"1,001il:0. N. C. 27,401
TC:I.C., .. ◊,.C .tio/376·6200
l'CLCCOPtl.'.:A \;IIP/370/41:0'-d
w"'.Sl·HNGTON 0. C. OtFICC
MA<1.tN0 A00AC9S
POSl Otf'ICC aox o()a:l:<J
WA:ININ0T0r~. 0. C . .20035-.6826
SUITC 120r.
TE'.LCPHO"'I: :.002t77Q-0'='$0
TC.~i:;CO~ICR 1!021-42;;1·61-410
I am writing in reference to our conversation earlier today. I
need to obtain copies of pretreatment or discharge permits that may
have been issued to Cristex Corporation or IMI between 1965 and 1986.
You may forward any infonnation to the above address. If there is a
copy charge please enclose the invoice with their.formation.
I appreciate you assistance on this matter.
Sincerely, -,
JJ~~ -&~
Glenda L. Barton
office Assist~nt
r·1AY 22 ·92 12:43 ~;f•11TH .115 F:HLEIGH
TELECOPY TRA!ISMITTAL YROM
I-
I SMITH HELMS MULLISS & MOORE
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I COMPANY:
ATTtMTION:
I FROM:
NUMB!:R or PAGES
I DAT!::
I XESSAGt:
Attorneys at L~w
Jl6 West Edenton Str••t
Raleiqh, North Carolina 27603
W93 -;1./..9 /
Telephone [phone]
Telecopi•r 919/828-79J8
ZapNet 919/832-0287
-~
(INCLUDING CO'/£R i'AGE):
5 -;);;J -9<?)
IF YOU H.\Vt ANY PR08L£MS RECEIVING OR DO NOT RECEIVE >.LL PAGtS, a PLEASE C.UL (9l9) 828-8207 ANO ASK FOR ""'~°"""'tvrl""c.;...;~d.o__)=..::=--------
I THE !NFORMATION CONTAINED rN THIS FACSI!-!ILE !-IESSAGE rs LEC>J.LY
CQt{PIQelfl'IALITX NOTIC?
PRIVIL!:Gto ANO CONFIOtlITIAL rNFORM>.TION INTENDED ONL'l FOR T}!f USE o ot TH!! INOIVIOUAL OR !:NTIT'l NA.MED ABOVE. If THE R.E>..OER or THIS
MtSSAGt I:S NOT nm IHTENOEO RECIPIE.N.T. YOIJ ARE HEREBY NOTirn:o no.T
ANY DI:SSDlIN'ATIOM, OISTRISliTtON OR COPY OF THIS FACSIMILE: IS n STRICTLY PROHIBITlO, IF 'lOU HAVE RECEIVED THIS FACSIXILE IN !:RROR,
PL0.51! IMMEDIAT?t't !40TIFY t:S BY T!LEPHONt A.ND RETURN TIit ORIGINAL
MESSAGE TO US AT TH? ADDRESS ABOVE VIA THE ~'NITED STATES POSTAL 0 StRVICE. TH>JQt YOU.
F'.l/2
I 227 »ort~ 1'1:yo~ street
Charlotte, lie a1202
tel•phono 704/ .l' 1-2000
l615 L streot, N1f
suit• 120$
100 H, Or•en5 Street
suit• 1,00
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••1ainqton, cc 2003,
T•l•paono ;OZ/77C•O55O
areenal:>¢ro, vc 27420
Tol•phone tlt/371•5200
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T1_1e City of Oxf c ~d
122 Williamsboro Street
P.O. Box 1307
Oxford, North Carolina 27565 FAX SENT
019-693-2195 (Voice) 919-693-149 l (Fax)
DATE
-
1-27-92
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TIME FAX NUMBER
For Ms. Glenda L. Barton, Office Assistant
Smith Helms Mulliss & Moore
Attorneys at Law
TOTAL NUMBER OF PAGES 4
FROM
Jesse A. Sullins, Jr., P. E.
City Engineer
-·--
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Permit No. 0106
CI TI CF CKFDRD
DEPARJMENI' OF fUBLIC w:::JRKS
WASTEWATER DISCH~ PERMIT
In accordance with all terms and ccndi tions of the Oxford City code,
Part II, Section 23, Article 11, et. seq., ard also with any applicable
provisions of Federal or State law or regulation;
Permission is hereby granted to Cristex Corporation
Classified by SIC N::l. __ __,2~2~5-=6 ___________________ _
For the ccntribution of _.=I:..::n=d=u=s-=t-=r-=i=a=-l_W=a-=st=ew=a-=t-=er=--------------
into the City of Oxford sewer lines at the industrial sewer line
This permit is granted in accordance with the application filed on
June 6 , 1984 in the office of the City Manager and in conformity
with plans, specifications and other data submitted to the City in support
of the above application, all of which are filed with and considered as part
of this permit, together with the folla..,ing named ccndi tions and
re::iuiranents.
Effective this 17th day of July, 1984
To Expire the 17th day of July, 1989
City Manager
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ADDENDUM I
Monitoring Schedule:
Self Monitoring -rronthly
Sheduled Mcni toring - 1 event per year
Unscheduled Monitoring - 1 event per year
Demand Monitoring -as needed
ADDENDUM II
Ccrnpliance Schedule:
Permit No. 0106
Permit No. 0106
(iy
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Parameters Cma/1)
Aluminwn-<lissolved ( All
Antimony (Sb)
Arsenic (As)
Bariwn (Ba) ·
Boron (B)
Cadmiwn (0:1)
Chromiwn-Total (Cr)
Chromiwn-hexavalent (Cr+6)
Cobalt (Col
Cooner (Cu)
Cyanide (CN)
Fluoride (Fl
Iron (Fe)
Lead (Pb)
Manganese (Mn)
Mercurv ( Mq)
Nickel (Ni)
Phenols ( Total
Saleniwn (Se)
Silver (Ag)
Titaniwn-<lissolved (Ti)
Zinc (Zn)
Total Kieldahl Nitrogen (TKN)
Oil & Grease (Petrolewn &/or
Phosphorus
Total Dissolved Solids
Temoerature-rnaximum <d=rees
pH-Maximum (pH units)
pH-Minimwn (pH units)
Biochemical Qxvqen Demand
Chemical OXvaen Demand
Susoended Solids (total)
Flow -(MGD)
E -Enforcanent Monitoring
SV -Surveillance Monitoring
SC -Surcharge Monitoring
mineral)
Cl
Pennit No. 0106 --
Limitations m
Wastewater Strength
Maxirrum Maxinum Moni taring
Cone. Instantane--R~ire-
(rrg/1) -oos Concen-ments
24 Hoor tration
Ccniposite (rrg/1 l Grab
Sanple Sarrple (E, sv, SC)
2.0 sv
0.1 sv
0.4 sv
0.5 sv
50 sv
3.0 sv
100 sv
5.0 sv
9.0 sv
6.0 sv
250 SC*
750 SC**
250 SC***
0.085 SC
* (1,000 rrg/1, Max.)
** (2,500 rrg/1, Max.)
*** (1,000 rrg/1, Max.)
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OFFICE OF THE
CITY MANAGER
To:
From:
Date:
Subject:
CITY OF OXFORD. NORTH CAROLINA 27565
1 22 WILLIAMSBORO STREET. P O BOX 1 307 -(91 9) 693-2 1 95
Daniel F. Finch
City Attorney
H. T. Ragland,
City Manager
August 17, 1992
MEMORANDUM.
Enforcement Action Against Cristex Corporation
Enclosed are copies of correspondence between Cristex and the
City concerning closure of the existing lagoon at the Cristex
Plant.
Please take whatever enforcement action that is necessary to
affect the closure of this lagoon and to bypass the normal
domestics sewage to the city of Oxfords' System. .
1.c;. ~ ~ ,'1(/V/tvr /a ~ r 04~1&fc/JJ> .
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OFFICE OF THE
CITY MANAGER
To:
From:
, '
CITY OF OXFORD, NORTH CAROLINA 27565
1 22 WILLIAMSBORO STREET, P. 0. BOX 1 307 -(91 9) 693-2195
Jim Cross, Attorney
Royster, Royster, Cross & Thorpe
135 College Street
H. T. Ragland, Jr., City Manager
Date: October 14, 1992
Subject: Enforcement Action Against Cristex Corporation
*************************************************************
Enclosed are·copies of correspondence between Cristex and the City concerning closure of the existing lagoon at the Cristex Plant.
Please take whatever enforcement action that is necessary to affect the closure of this lagoon and to bypass the normal domestics sewage to the City of Oxford's System.
P.S. I will review with you as needed.
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illitl! (©£ ®xfarb
OFFICE OF
CfIT ENGINEER
Mr. Shane McCarthy
Raleigh Regional Office
DEM -DEHNR
3800 Barrett Drive
Suite 101
Raleigh, NC 27609
Dear Shane:
April 22, 1993
Enclosed are copies of correspondence and other information
concerning these lagoons at the Cristex plant located near Oxford. As
you can see from this correspondence, the City of Oxford is attempting
to have this lagoon closed out. We are going through a selection
process now to get an out-of-county attorney to proceed with closing
this lagoon.
If you have any questions, please call.
JAS,JR/clb
Enclosure
CC: H. T. Ragland, Jr.
Tommy Marrow
fol/~/
Jesse A. Sullins, Jr., P.E. & R.L.S.
City Engineer
300 Williamsboro Street -P.O. Box 1307 -Oxford, North Carolina -27565 -Phone [phone] IO -Fax [phone]
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filittr ®£ ®xforO
OFFICE OF 77!£
CITY MANAGER
April 23, 1993
Mr. C. D. Malone, President
Hydro Management Services, Inc.
P. o. Box 1279
Clemmons, N. C. 27012
Re: Cristex Lagoon
Dear Mr. Malone:
I have had the occasion to review some of the history of
the problem of the Cristex Lagoon which still constitutes a
problem to the City of Oxford from the stand point of
Wastewater Treatment and reporting to NCDEM. Although we
have made some attempts to secure legal services in an effort
to bring to a conclusion the need for closing out this
lagoon, nothing significant has happened.
On October 9, 1991 I wrote a letter to Mr. George J.
Christensen, Jr. and notified him that he should take the
necessary steps to eliminate the overflow discharge from the
lagoon to the Oxford Sewer Collector System. In the letter I
notified him that we would take action on the matter on
November 1, 1991. Since that time nothing really has
ha~pened and I now feel that we need to move seriously to
bring this matter to a conclusion. I do intend to discuss it
with the Mayor and Board of Commissioners in the next regular
meeting in an Executive Session. In the meantime, I would
appreciate it if you would give consideration to this matter
and give me the benefit of any information that you may have
concerning an attorney that would be willing to handle this
matter. I am convinced that neither our City Attorney or any
local attorneys would want to handle it due to the fact that
many of them are associated with the Committee of 100 which
is very supportive of Industry. While they are supportive of
Industry, it appears to me they have no interest in entering
into any matters which might be controversial in so far as
industry is concerned. Therefore, it remains that I must
take the initiative to deal with this matter.
I would appreciate any ideas or any suggestions that you
may have on the selection of the attorney to include the
naming of any individual that you feel comfortable in
recommending.
I tt;rely,
1/~ l;M/J
-Ragland, ;_.. /
I City Manager ~
.-3-00_W_i_ll_ia-n-,~-:-o-:-:-:-:-:-e~-~-~-,_-Q ___ B_o_x_l3_0_7 ___ 0_x_fo_r_d ___ N_o-,1-h_C_a_r_ol_in_a ___ 27_5_6_5 ___ Ph_o_l'_.e_(_9_19_)_6_0_3 ___ 11-0-l---l-,,-,x-(9-l-9-)-60-~·-
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State of North Carolina
Department of Environment, Health, and Natural Resources
512 North Salisbury Street • Raleigh, North Carolina 27604
James B. Hunt, Jr., Governor Raleigh Regional Office
April 15, 1993
Mr. Charles B. Royster
Environmental Affairs, Revlon
1501 Williamsboro Street
PO Box 6111
Oxford, NC 27565
Subject: Discharge of Oil
Cristex Corp. Building
Granville County
Dear Mr-Royster:
Jonathan B. Howes, Secretary
OTY OF OXFORD
0 Alf -NO RESPONSE
0 Alf-W/COPY REPLY
APR J 9 1993
0 COPY{IES) TO
D Rf.ROUTE TO
0 RE.SPONSf ON TAPE
On Sunday, March 28, 1993, Mr. Shane McCarthy of the
Raleigh Regional Office (RRO) responded to an emergency
management call concerning an oils spill at the Cristex
Corporation Building, located on Industry Drive. An
initial estimate of 14,000 gallons of number 6 fuel oil
was discharged from a storage tank located behind the
Cristex Building. Fuel oil from the tank was released to
a storm drain near the bulk storage tanks which then
drains into an abandon aeration pond. Cleanup activities
were implemented at approximately 1:00pm the same day and
staff from the RRO reinspected the site on Tuesday, March
30·, 1993.
At the. time of the investigation it was unclear to
Mr. McCarthy which party was responsible for the oil
storage tanks after speaking with representatives from
both Revlon and Cristex. In an effort to examine the cause
of the spill and to determine the possible responsible
party, the RRO is requiring a written response outlining
the sequence of events that led to the discharge of the
oil. Please include in the narrative; the name(s) of the
contractor(s) involved, any documentation as to -who owns
the tank as well as who is responsible for maintenance of
the tank.
While your response should at a minimum include these
items mentioned .above, please feel free to add any other
information you feel is necessary. Please have your
response completed and postmarked no later than April 30,
1993.
3800 Barrett Drive, Suite IOI • Raleigh, N.C. 27609
Telephone [phone] • FAX Number [phone]
An Equal Opportunity Affirmative Action Emplo}"'r
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Mr. Clarence B. Royster
Page_2
April 15, 1993
A similar letter has been sent to ·Cristex requiring
them to submit a response documenting the same type of
information.
If you have any questions please feel free to contact
Mr. Shane McCarthy at 571-4700.
cc: City of Oxford
Sincerely,
?~~~
Timothy L. Donnelly, P.E.
Water Quality Supervisor
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MEMO
DATE:
TO:
FROM:
SITE:
April 21, 1999
File
Jeanette Stanley
Environmental Chemist
NC Superfund Section
Cristex Drum Site
NCO 001 606 250
~
Oxford, Granville County, North Carolina
Ref 18
A file review was conducted on Air Quality files. The findings are summarized below and
the files are attached.
A February 15, 1973 inspection resulted in the filing of a Request for Registration of Air
Contaminant Sources (fom1 AQ-1) and an Application for Registration of Fuel Burning Equipment
(form AQ-2) for the two 600 hp natural gas boilers with #6 fuel oil standby. The facility was in
compliance at that time (pp. 1-5). On August 30, 1973, the facility was inspected and both stacks
from Tenter Frame No. I (placed in service in 1966 (p. 14)) were in excess of 80% opacity (p. 6-7).
[ A tenter is a framework on which cloth is stretched prior to dyeing, for drying without shrinkage
(Ref. 32, p. 295).]
On February 19, 1974, a plan of proposed actions to control visible emissions was submitted
to NC. The plan included construction a multi-stage oil mist collector and electrostatic precipitator
for particulate and smoke removal combined with an energy recovery system (pp. 8-l 0). On March
18, 1974, North Carolina issued a temporary permit (No. 2428) for continued discharge until June
I, 1974 (pp. 11-16), pending adherence to the construction of emission controls.
On April 19, 1974, !MI Warp Knits, Inc. submitted the application for construction and
operation of said air pollution abatement equipment. After a May 7, 1974 inspection and review,
North Carolina recommended issuance of the permit (pp. 17-37). On Nov. 24, 1974, !Ml requested
an extension for construction, and on Dec. I 0, 1974, NC granted the extension until April 30, 1975
(pp. 38 -43). On February 17, 1975, NC determined that the contract for construction had not yet
been let (pp. 44-45). On March 11, 1975, another extension was requested (pp. 46-47). IM! Warp
Knits reported a reduced availability of natural gas and economic problems.
A Special Order by Consent (AQ-75-055) was issued· on August 12, 1975 to extend the
compliance deadline to October 30, 1976 (pp. 48 -60). Another extension (I 8-months) was
reg uested due to financial expenditures to update the facility (pp. 61-63). The estimated cost of
installing the pollution control equipment was $70,000 while the estimated cost of necessary updates
was $1, I 00,000. These updates were to install nylon beaming equipment (p. 65). In May 1976, the
NC Air Quality Section denied the request to extend the October 30, 1976 deadline (p. 66).
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Memo to File
April 21, 1999
page 2
A permit application for operation of six atmospheric dye tubs was submitted on January 5,
1977 (pp. 71 -78). A February 3, 1977 inspection indicated that, while construction was not
complete, the requirements of the SOC would be met with completion (p. 79). A request for renewal
of permit No. P-2097 was made on October 17, 1977 (p. 81 ). A November 15, 1977 inspection
showed that the unit was still under construction and that additional emission sources needed to be
added to the permit. By January 19, 1978 applications had been received for all emission units and
the emission control device was completed and in compliance (p. 83).
A May 23, 1978 inspection resulted in the issuance of a Notice of Violation for exceedence
of visible emissions (pp. 84-86). An application for continued operation of tenter frame No. 2
without pollution control equipment was denied (p. 87). Permit No. 2097R was issued on July 28,
1978 for the six atmospheric dye tubs, two no. 6 oil-fired boilers, the No. 3 tenter frame, and the air
cleaning device for tenter frame No. I (pp. 88-103). A May 23, 1978 inspection showed that the No.
2 Tenter frame exceeded visible emission standards (p. 104). Options were pursued to meet
compliance, and Permit No. 2097R2 was issued on February 23, 1979 along with an SOC-mandated
compliance schedule on May 10, 1979 (pp. 105 -127).
A compliance inspection was conducted on July 17, 1979. The equipment was installed but
was malfunctioning and a followup visit was required (p. 128). August 9, 1979, July 1980, and
December 1980 inspections found the units in order (pp. 129-132). Permit No. 2097R3 was issued
on June 26, 198 I and was valid until April 1986 (pp. 133 -146). In a report dated March 2 I, 1983,
an Air Quality Permit inspector noted that exterior emissions were in compliance but questions
regarding a large amount of smoke inside the plant were unanswered by plant personnel (Ref. 12,
p. 4).
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,:!JI . , ' .•.·' ·'·.' •. •••.· .. :·.• ...... ' ~· ~.-:• J:..f,._,/ -/. ,~.'::, __ ,,... ......
AIR QUALITY DIVISION J-/JC /(),::,. ,.,,-.:..··./··i;,'.?·::
REQUEST FOR ACTION TO BE TAKEN tx;', ... ; ,/
The item listed below requires action to ascertain compliance under Article 2Y: Chapter 143 of the
General Statutes of North Carolina, concerning rules and regulations governing the control of air pollu•
tion:
Name
Subject
lllI l•:arp Knits
Address O:cfor1
Engineer eVulu~tion and regi3tration
Investigation Requested By
Central Region
Remarks
New Source
Assigned To
Centr i:1 Region
Irlvestignted By
Melvin Flora
Action Recommended
Compliance as per report
Investigation Report
Address
Raleigh
Date
2/15/73
t. Contacted -Hr. Jack Stanley, plant ma.na1cr.
Lir. Jim Pa::terson, plant_ cn-2:L1ce~.
Hr. Fred Jeron:l.mus, technical advisor.
2. Engineering evaluation
a) two 600 hp boiler, ncitural gas with ;'/6 fuel oil standby
b) nolid waste -connnercial pick up
c) proc0ss -knitting; dyin,; and fininhing
d) water based dy0s
County Granville
County
Date
2/13/73
Returned
2/21/73
e) non.areactive finishing solutions (mela.~ine resin and methenal)
3. Registration -assisted in filling ~ut AQ-1 (to be mail0d)
4. This company in compliance with all standards,
Correspondence To: i ·' :.,'
Signature:
White-Engineering Branch; Yel1ow-Central File; Blue-Regional Office; Green-Engineering Branch
AQ-16 Rev. 7-1-71 (9
LI., ~C-0 _)Q'_!:•(/L.A'l-)/_ I 4-
f, 111,::r !))cvrf /'(n<fe ~--ru::..-
NORTH CAROLINA DEPARTh\ENT OF NATIJRAL AND ECONCMIC RESOURCES ~~
Office of water and Air Resources
Air Quality Division
P. O. Box 276ITT
Raleigh, North Carolina Z/611
{Three Copies To Be Subm: tted)
{Fourth Copy Should Be Retained By Applicant} RECD FEB 1 g 1973
REQUEST FOR REGISTRATION OF AIR CONTAMINANT SOURCES
In accordance with prov1s1ons of regulations of the Board of Water and Air Resources,
application is hereby made for the registration of equipment which emits contaminants
into the outdoor atmosphere. I+======~~-~-----+
lA.
I f U T llllnn lll\11 .... (llr-\ TNr
l----------------=B.:u.:s.:i.:n.;.e.;.sc,s_;Lc..lc.,c:.:ec.n=i'e...:.:N.:am'-e"--'o:.:f--=O.:r-'g-=a.:n.:iz:.a:.t __ i.:oc.n;_;T.:.h.:a.:.t--=.Ic.s_T:.;o;...:8:.:•;__;_R.:•-"g-=ic.st--•=-r:.:e:.:d _______________ -1
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18,
-. .... . .. .. "' .. '" sl tners Doino Business as Above Oroanization
2A. Mailing Address: 28,
. . ..
Numberlr1u1.1:,, Lr y u1 1 ~reet u s uQ1 VI 111a Code
3A. Equipment _Location Address:
-..
Numbe VY C:;treet Zin Code County Phone
4. Equiprr.ent To Be Registered (Check Appropriate Installation(s): for each Indicate number of different (nonidentical) units
Fuel Burning Equipment --------~'-·--':z''--
Incinerators ------------------tJ g
'2--2.
I Gas Cleaning Devices----------□,--,,--
! ______ ..:.rn~d~u~(s~t~r~i~a!l~P:ro~c~e~s~s+o.ir~Mjai,nii_ufa!.c~tju;;rii~n~g~Q2qiu~,· p;m~e~n~t~:IJ:eiJ§E~!EliJi;:Jlli:::;==:J~il:li===========::t f Pulo and Paoer· Textiles Minina. Furniture &I 1-lietals. Etc. Sneci fy
I -4.
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5. Type Organization:
Corporation---------□
Partners hi p---------fS]
Individual Owner----□
Government Aoenc ,---0
6A.
Sian u:te Rifso~i"ble efen1'oer of -;.;.'ation
DO NOT WRITE IN THIS SPACE
C Registration Number Coordinates
3
6B,u~ -•• · ·--
OHiC.i.ril T1t1"' o1'~Icfner'' !j"•
2 'Ui '73 I a i . --. --.....
' 1~6,¼-~mh'e~ ~ I
• ·s: >-a c
Date Received Regional Office Date Received State .
>-0 ~. ·-. -C, .--6
Date Applications Forw~d 50 APfil7'3nt Reviewed By· 7 Date
Date Applications Received From Applicant Date Applications Processed
Comments:
Centra!
ROBERT W. SCOTT
GOVERNOR
If ALES W. BRADSHAW. JR.
SECRETARY Office of Water and Air Resources
GEORGE E. PICKETT, DIRECTOR
TELEPHONE [phone]
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oate __ M_a_rc_h_l_9~•\{._.£..,...9.( ..... ,q..,.~-.!b~?,~'2,~?.,. ___ _
Firm_~I~·-M~·~I-~W~ar~p_Kn_i_t_s~(N_C~)_In_c_. __
Location Oxford, North Caro 11 na 27565
City -----------------
Application is hereby made to the North Carolina Office of Water and
Air Resources for the "Registration" of the following installations as required
by the "Rules and Regulations Governing the Control of Air Pollution in the
State of North Carolina."
Installation (s)
Type of Installation Number of Ea ch
600 H.P. Cleaver Brook 2
. '·
Signature,.µ~::._\Ld.:.._--1,iJ' ~'~:::!::'.::::+---
/
Cer1traJ \
~ iJ\~y
AQ-10-12/15/71
IIVISION OF DIVISON OF DIVISION OF
IA QUALITY WATER MANAGEMENT WATER QUALITY
DIVISION OF DIVISION OF DIVISION OF
GROUND WATER WATERWAYS & SEASHORE PLANNING
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l. Owner of Installation
I.M.I. Warp Knits
Mailing Adciress
Industry Drive
City
NORTH CAROLINA OEPAR1MENT OF NATURAL AND ECONOMIC RESOURCES
(NC)
Office of Water and Air Resources
Air Quality Division
P. Q. Box 27687
Raleigh, North Carolina 27611
(Three Copies To Be Submitted)
(Fourth Copy Should Se Retained By Applicant)
APPLICATION FOR REGISTRATION OF FUEL BURNING EQUH-MENT
Date of Application
Inc. 3-19-73
Telephone
919/693-6141.
State Zip Code
RECD MAR 2 2 1973
DO NOT WRITE IN THIS SPACE
Date Rec. Reg. JDate R~~-State
"'" ' ".l 107'.\
Acknowledgement Sent:
Date By:
Reviewed By:
Name Date Oxford N. C. 27565 Rea. I I
2,. Applicant or Authorized Agent Telephone State I I.
DNA Copy to Reg. Eng.
Mailing Address City State Zip Code Date:
Application Returned to Applicant:
3, Location of Fuel Burning Equipment City state County Zip Code
Date: By:
4, Installer or Contractor. (If New or Replacement) Telephone Registration Number:
Applied Engineering Co. 919/275-1631 R-
Mailing Address City State Zip Code Coordinates
807 Winston St. Greensboro, N. C. 27405
5, Starting Date (New Installation): Completion Date: Date Existing Installation Class Number
-Placed in Operation:
I Feb., 1971
6, Si ana ture of Ownnr ~uthorized Company Official Title Print or Type Name Title
/I J (J .1! n, ., . Plant Mgr. Jack H. Stanley Plant Mgr. • /,-f . V
7, (Jpe of Regis tr~ tTon V 8, Major Activity at this Location (Check One)
Existing Installation Altera tion--------O ... Manufacturing---------~ Hotel or Motel---------O
(Initial Reg,)-----------19
Addition----------□ Retail or Hospital---------------O
New Installation Wholesale Store------O
(To Be Constructed)------O Change of (All 1ypes) ----□
Warehouse--------------O
Ownership--------0 Office
Replacement---------------O Apartments
School or Church------O (Over 4 Units)--------O
Other D Specify Other
Specify 0
g, Identical Installations at this Locat~n 10, Name of Fuel Supplier · Address Telephone
2 as Public Service Co. of N. c. -Henderson, N. C. 438-819i
Number of Units 011 Amerada Hess Coro. Soartanbur<'-S. c. 803/582-5301 -
11, Stack Height Above Ground Level (In Feet)
30 feet or LesS-------O 31-50-:--2----~ 51-100-------[l 101-150--------0 l 51-200-------0201-250-----[)over 250-----0
12, Specify Type and Amount of Each Fuel Consumed Annually in this Installation:
Coal--------0 Tons Oil--------□ 71,000 Gals. Natural Gas---------d cu. Ft,
Wood--------D Tons Other------□
r'\ Specify and Amount . -
13, If Oi 1 Is Used, Check All Grades Applicable: ~-e1-1_[ I r a , ___ -,!Q ~() ,,,
No, !---------□ No, 2-----------□ No, 4---------0 N --j ~err , , · .
...,, f I
-AQ 2 6/30/71
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14. Type of Oil Burner
Pressure or
Gun Type------------0 Rotary Cup----------0 Steam Atomizer---------O Air Atomizer-------~ Other----O
Specify I
15. Type of Coal Burning Equipment Used
Hand Fired-------------0 Spr_eader Stoker---------0 16. Fly Ash Collection Equiprnen t
Underfeed Stoker-------□ Stoker Fired with None---------------0 Electrostatic
Ash Reinjection--7-----0 Precipitator--------~
Traveling Grate--------0 Cyclone------------0
Scrubber---------~~---□ Pulverized Coal---------0
Chain Grate------------0
Furnace---------□
Multiple Cyclone---0
DNA Cyclone Water Spray" in
Other 0 Settling Chamber Stack----------------0 Specify or Baffles--------□
Other Inertial Separa-
TIA. Smoke Indicator in Stael< Other--------------O tor (Tubular, Cone, .
No-------ltl • etc.)----------------0 Yes-------0 Type
Specify · Describe
17B. Are Oil ---------.. -·-··----·-.. 7 Heaters Used 18. Amount of Fuel Consumed Annually in These Units Only
Yes-------[X No-------OTempera ture J.ZLo F Oil 71,000 gallons Coal tons
Natural Gas
19A. Sul fur Content of Fuel to Nearest 198. Ash Content of Coal
Tenth of One Percent Ash
Coal % Oil 2. 1 % 19C. Specify Method and
Lancing------O
20. N,aximum Firing Rate (BTU Per Hour Input and Hourly Feed. Rate).
Input 25,106,000 BTU/Hr. Coal
Wood Lbs./Hr. Other
21. Stack Emissions From this Installation
Particulate Loading !Jnkno!lln
Flue Gas Volume
Sul fur Dioxide
Carbon Monoxide
Emissions From This Installation:
Sul fur Dioxide
Particulate Matter
Oxides of Nitrogen
Hydrocarbons
Carbon Monoxide
Other
6/30/71
Pounds
Lbs./Hr. Oil 167,5
Specify
.
Gr./C Ft.
C:-M Of
Lbs./Hr Oxides of Nitrogen
Lbs./Hr Hydrocarbons
00 NOT WRITE BELON LINE
Per Hour Pounds
-2-
Cubic Feet Other I Specify Amount
to Nearest Percent
%
Schedule of Tube Cleaning, If Applicable.
Tube Blowing-------~□ Schedule
Sneci fy
Gal ./Hr. Gas cu. Ft./l-lr.
Lbs./Hr.
In. Hg.
Lbs./Hr
Lbs./Hr,
I
Per Day Annual I
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[i / ;') :/ ;". . / ·/:j'-;; -··· ,, ,· --1· (.,' ,. '-'
REQUEST FOR ACTION TO BE TAKEN
The item listed below. requires action to ascertain compliance under Article 21, Chapter 143 of the
General Statutes of North Carolina, concerning ·rules and regulations governing the control of air pollu-
tion:
Name
I,!·;, I. Wa::p ,:nits
Subject
cn~i ~1--Jerirn· evaluation
Investigation Requested By
i~ent.?:ql "'n•!".;r_n
Remarks
Address
n,~f.·.··,·1
Address
County
County
Assigned To Date
tr\vestigated By Date Returned
:) /10 /-P q/'J 1 /73
Action Recommended
IIlvestigation Report
L. o~~•c::-vccl ,#1 t.2nt;:;~f:-.::n2 0£ I.E. I. '::Ja:-p l~-iits in c::COGS of ao~i~ opacit·j. ~his ~mission
W::15 confined to t:vo :Jtacks .:-emoving }?l:'OCess emission fro:n. zone 3 an<l 4 of the frame.
J. Is3ucd AQ-4 fm: tent.3:r frames and assisted with sane.
Correspondence To:
Signature:
White-Engineering Branch; Yellow-Central File; Blue-Regional Office; Green-Engineering Branch
AQ-16 Rev. 7-1-71
.'··•C.•-··/'" ....... , ......... --.. ·. -, ••·_ ... • ......... c:.·"
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(Three Copies To Be Subni lted)
(Fuurlh Copy sr.ould Be Retained By Applicant)
SUPFLE/:,:::NH.L DATA SHEET FOR REGISTPJ,TIO!! OF iJEY/ A:-rn EXISTlMG HJSTALLAT10NS
Firm Name
I. fl-/. I -w a,'-<A'J
Address This Ir,stallation /
City or Town J
0 ?(~-~---V
r;@~a~ID
AUG 3 0 1973
AIR QUALITY DIVISION
CENTRAL OFFICE.:-::
it :).
r --I
p 0 I ovo I
I Is: I
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l F ;
"00 P IQ I
'--_j
Type Installation
~ i
. r --f'o FdP
I o o I
f;~
! OFO t
V/51131.E (:'1·,·11'3'5/C;v'S
AQ·6 6/1/71
F 1• Ii_ 11·1 ;: :: I ;;'-ON £ 3 i '1-
i?, r.., -;· ~-51,:.;c k 5
?,C' 9o
Zip Code
FOR DIVISION USE ONLY
Date Received
Date Registered
Registration Numbe:-
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l,!'-1,I, WARP KNITS (NC) INC,
INDUSTRY DR.
OXF0RD,N.C.27565
TEL. [phone]
RECU FE82U 1974
Mr. R. G. Fore
Chief Engineer
Air Quality Division
February 19, 1974
Department of Water & Air Resources
Raleigh, North Carolina 27611
Dear Mr. Fore:
Enclosed you will find a status report of actions taken
to date to evaluate and control visible emissions from
our Tenter Frame #1. Please note the proposed changes
in the timetable for our pollution abatement program.
I believe that the schedule suggested by our consultants
is reasonable in view of our intentions to acquire a
system that will combine energy recovery with the
necessary smoke abatement technology. We request that
you extend the temporary permit in accordance with the
schedule contained in the status report.
Thank you for your consideration.
/ah
Enclosure
· Very truly yours,
<) ~'-'Ji ))o....1(,.1
l/ ~ack H. $tanl ey
Plant Manager
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The Hill Environmental Group
Post Office Box 659
Chapel Hill, N. C. 27514
Telephone: [phone]
Mr. Robert P. Clewell
Consultants in the Environmental Sciences
February 15, 1974
Industrial Engineering & Administration Manager
I. M-I. Warp Knits, Inc.
Industry Drive
Oxford, North Carolina 27565
·O Dear Mr. Clewell:
The purpose of this letter is to present a status report on the engineering
design of a heat recovery and air polluti~n control system for tenter Frame
No. 1 and a schedule for the remainder of the project. Our plans continue
to center around the use of a multi-stage electrostatic precipitator for
particulate and smoke removal and an energy recovery system to heat water
for use in the dyehouse. We estimate that from the No. 1 tenter frame
enough heat can be recovered to handle approximately 70% of the hot water
requirements for dyeing. It appears that the payback period for such a
sy'stem will be in the range of 3-4 years. The engineering analysis . is
near completion, and the actual system design and specifications should be
complete within 60 days. At that time the permit application•will be sub-
mitted to the Board of Water and Air Resources.
The following is a summary of activities completed to date_
(1) October, 1973 -Initial discussions between I. M. I. Warp Knits and
THE HILL ENVIRONMENTAL GROUP, Proposal for source testing submitted
and accepted.
(2) November, 1973 -Evaluation of visible and particulate emissions from
tenter frames 1 and 2.
(3) December 5, 1973 -Report of results of emission studies.
(4) December 27, 1973 -Proposal for design of energy recovery and air
pollution control system.
(5) January 10, 1974 -Contract awarded for design of energy recovery and
air pollution control system,
(6) January 20-21, 1974 -Engineering survey of tenter frame No. 1 and as-
sociated equipment to gather data on tenter frame,burners, fans, ducts,
building structure, etc.
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hr. Robert P. Clewell
Page Two
· February 15, 1974
We are presently in the process of completing the engine~ring analysis,
establishing the size, weight and configuration of the equipment, and
preparation of construction drawings and perfonnance specifications •
. These activities should be completed within 60 days.
The following is a proposed schedule for the completion of the pollution
abat~~ent program for tenter frame No. 1.
(1) April 15, 1974 -Submit plans and permit application to Board of
·Water and Air Resources.
'!'iote: The Board inay take up to 90 days to review plans and issue
·permit. For this timetable, it is assumed that a permit will be
· issued within 30 days.
(2) May 15, 1974--Permit isqued. Prepare contract documents.
(3) May .22, 1974 -Release bid packages •
. (4) June 17, 1974 -Receive and review bids.
(5) June 24, 1974 -Award contract for control equipment.
Note: A minimum delivery time of 16 weeks is assumed;
(6) September, 1974 -·Basic mechanical and electrical preparations for
installation of equipment.
(7) October 24, 1974 -Delivery of contr_ol equipment. Allow 21 days to
install •
(8) November 16, 1974 -Final installation and start-up.
(9) November ·30, 1974 -Performance_ testing and final acceptance.
The above schedule should be submitted to the Air Quality Division with a
request for amendment of the timetable contained in the Application for
Temporary Permit.
Very truly yours,
THE HILL ENVIRONHENTAL GROUP
Grover C. Wrenn, Jr.
GCW/cmg
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Hr. Jack H. Stanley• Plant Manager
I.H.I. lfar:, Knits
·Industry Drive
Oxford, North Carolina 27565
Dear Hr. Stanley,
March l8• 1974
Subject I Ter m:acy-2ei.mit_No. 2428
.H.I. lfarp-~
Oxford, North Carolina/ ------------' 111 accordance with your application dated A1.:gust.JC, 1973, ve are
forwarding he1.•ewit..:.'l Tenlpor~u·y PctTuit no. 2428 dated 1•.i.arci1 18, 1·)74 to
I.H.I. War'? ~:nit:;i, Oxfor<l, North Ca~olin.a for the continued discharge of
air conta-;;inant·s resulting from orocc,;s operations at its facilit.y located
a·t Oxford, North Carolina, Granville County, until provisions for t:he correction
of the proce33 cperations can be e~tablinhed. ·
This Tciaporary Per.nit shall be ~ffective from tho date of ita issuance
until June l, D74 and ahall ue subject to the conditions and lii:titations
as specified therein,
Sincerely yours,
.t.. c. Hubbard
rtGF1go.
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; :: :~ :i,_,,.-, :.:.
NORTH CAROLINA
BOARD OF WATER AND AIR RESOURCES
Raleigh TE~tQni\E%
·.~.~
j 1 ;~ -\~'.,
For the Discharge of Air Contaminants Into the Atmosphere
In accordance with the provisions of Article 21 of Chapter 143, · General Statutes of North Carolina
as amended, and other applicable Laws, Rules and Regulations,
PERMISSION IS HEREBY GRANTED TO
I!·ll '.-Taro t{.nits
O,:ford, North Cai:olina
FOR THE
continued discbar3c of ai:: cont,1:minnntz ro.c.ultin:~ from ::.'lror.:.cs~
o:1crations ot its f..1::ilit7 located nt 0}:ford, i·iorth G.:1:-0lina,
<Ji-anvillc Count1, until ?t"o~1iJion3 for thn corr"Jction of the
lJrlJccs.s operations -can be established,
in accordance with the application dated •' ,·:,.,.,-.,,., 19----7...l_, and in conformity with the
plans, specifications, and other supporting data, all of which are filed with the Department of Water
and Air Resources arid are considered a part of this Permit.
This Permit shall be effective from the date of its issuance until --'-·-··~•n~'~---~19....1..'.,_, and
shall be subject to the following specified conditions and limitations:
. :"sy .run(.! 1, L)7!i,., ·r:·.1 ~1:i::;, ;,~nit:1 :;h;:lli ::'~due:.,~ Vi::;i:.)lc: ,:i.n·J rr.1r::.icu~,}t:1 cr:1i;;:-;io1rn !::J
l,~·1cls n~ ·J!:'".}ater thaa ~1c1.·:,titt.:!d '.J"J o~pli-.:.:.J::ll•:J 1."".:!~;1.~iation::; o:..· -:;t.:1nd;:i=~l;; m1d ;;hall
n:-i!;13r2 to che .Eollo\,;in;3 ::ow~1li:1n-:.e. schc-:iu!.t.:!:
l.
, . . .
-::vnt::::ict(s) fo:-er.:i:;Gion .-:ont~oL; uill ;).~ nuo.:::lc.J b--; -::u·: l i, 117!4 •
,;;o;i:-:; t::-u:::.tion ~.vii l :Jt1 iic:,;un Yf i'-:-:1'1 L 5, l ')7 1.-. • •
?.1.cili::ics will '.J:, cvr::?ln.tcd and !)laced i:1 o:K?r:ition 'J7 .June 1, 1')7 · ...
'.:)uriag th-2 :Jc::-ioti of thi·J 2cr.:po.::-3i7 ;?on::it, .'.l ::1rcg:~·c:~:i· ::-.'"}7::0~~ :ih,.-ill :,o filed ~ .. ;ith
thiJ o:'.:ficr/ ::it Juch intc::-voln ~nd in {;uch fo~c7 ::in.:i detail ,:J.::i r:::.:..1-,, be :"CriUi.1.·Gd '.J?
!:h•~ Bon::-d or it:; :idwiaiJt::ativc :3t.:1ff. ·
Notice.: i'hi::1 !cmpo::a...-"f I>errait shall not ~c construe•.l t:o authori .o tltc c1.~eatiun at· ::-.~-1in-
ten;;!n~c of n aui.Jnncc. ~\.lso, it -..~ay be ::evoked bc,:.'.l;.i~1a of fJilu=c to ;JroviSe 8.0di£i:::::ition
..J:° tlro.;c·.::•: r.n':'t:::iti:•m.s and/or runL;sion control i:.-1~ili~ic.:; i:,, .1c~ot·:iani:..:!-"W'it.h the: :i:.>o·,e set
\::.a;:-i{iitionfj. !'hi~ docu:.-.:unt i:1 sub.Jc¼-t to ·,1nli:! lir.iitatian::; of ar..:1 loc.:il, -:-,ri"'.'-:ltC ,n· !';I)CCiu:
~,:t O!" ::c!;olution ::-~l..1tcd to r~c:ilth, ~anit:J.tion or a.bat~t:,G.nt of nui:J.o.n~CT:.1. It i.3 not in-
tended no:: .,-,;h::ill it Je ~o:1:1trucd to c..::-c.:1tc, •:::.onfar, ··:-.c::rr.it or ,1;,1)ro~1,~ ::.he ~:t(''.r~i:.:;c of ,:ur, ::1;,_~ht, 7.10:101·, ;1rivilc:1e O'i:' ir::ri.unity whi.~h ma?· :Je :oz'.Jiddcn ::i:, tht! valid ~Jrovi:;ion of any·
su:;h lo.-::11, ?ri~:atc or ·:,7.1eci4l act or-::a.:.iolution.
Permit issued this the 18th day of Harch 19-1!±....
NORTH CAROLINA BOARD OF WATER AND AIR RESOURCES
By
Permit No. __ 'l;'.:::2428_
Fr/I . . e /,.:-< ... .?.:_.~ ...... 7'--:__,_._.;,r---:,'__,--7-/
Assistant Director
Office of Water and Air Resources
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BO~D, _OF WATER A~D ~ ~, r ~ r
' Raleigh tJvTl t. ~ u E
APPLICATION FOR TEMPORARY PERMIT• ,
AIR QUALITY DIVISION
CENTRAL OFFICE
To Continue Discharging Air
Contaminan'ts Into The Atmosphere
-Fi!e Copy
Three Copies Jo Be Sµbmitted
Fourth Copy Should Be Retained By Applicant
To: Board of Water and Air Resources
• ·p. O .... Box 2704_8
Raleigh, North Carolina· 27611
In acco':i-dance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina
and _a~l~a~l~Julati_ons. C?.f the B<?~rd o_f Water and Air Resources, -application is hereby made by a t Y . of the · I.M.I. W Knits· · ·
_(N~me __ of Bo_~rd; ·i~d~vidual: or Others N_ame of city, town, ~ndustry or establishment
-in .the county of Granville , at __ Oxf=::,o:cro=-=---------------------
(Show post office, address or location)
f()I' ·permission to continue discharging into the outdoor atmosphere air cOntaminants resulting· from
visible-from tenter frame #1
Identify _source
1. INFORMATION PERTAINING TO PRESENT EMISSIONS:
a.
b.
c.
Waste
( 1).
(2).
(3) •.
Fuel
( 1).
(2).
(3).
( 4).
Disposal by Burning
Estimated quantity of·material
Type of material burned:
LoCatiOn of burning site:
Burning Installations
bu!'ned: ________________ tons/day.
FrequencY: -----------'------
Type of fuel used: _____________________________ ......,:
Quantity of fuel used per day: ________________________ ~
Fuel characteristics:, BTU Value_-=--,-=--,--% Sulfur ______ % Ash_'--_,
_Stack Height _______ ....;,,_; Stack Diameter --------------'--'
Industrial Process
(1). List product or _prod_u_cts_· __ N~y~l_o_n_A_c_e_t_a_t_e __ Kni_"Fs ______________ ....:......:
( 2).
(3).
( 4).
List qua n tr hes Of' prod u~ct_ or . prod UC ts produced -----'2.J.□La, .... sJ..laJ..la.L+l, n"'n""n"-y;,,.n=s.1../.;J.yr.i.;,,., _____ ...,
-----------------' Li st air contaminant"s emitted --""'-'j_,,5_,j.,_h.wJ1.teac..te"'mll.1,_,· s,.sii.w' 0.J."u.S.,,·------'---------' ~~-~~-----~------· Estimate the quantity of each contaminant emitted
exceeds 80% opacity ;
2. INFORMATION REGARDING PROPOSED POLLUTION _ABATEMENT ACTION:
a. Action Proposed: Comply with state standards
l). .Time schedule for accomplishing the yarious steps necessary to completing the proposed
pollution ·_abatement· program:
(1). · Engineers will be retained on or before Sept. 1 , 19 73 .
(2). Reports and plans will be filed on or before Feb. l5 , 19~
(3). Construction will be begun on or before Ma 15 19 74 .
(4). Facilities will be completed and placed in operation on or before June_) , _19-1!±.....:
3 •. 13TATEMENT OF AGREEMENT: (5) Contract let May 10' 191'+
The applicant hereby aggrees that the proposed abatement action will be carries out in
accordance with the proposed time schedule contained heI'ein, and 'further agrees to submit
progress reports at regular intervals as requested by the Board relative to steps being taken
toward accomplishing the necessa_ry pollution abat;ement measures ..
Date 8/30/73 Signed I.M.I. Warp Kruts
--,---,:( c"'i,.,..---;::-----:-;,---,,---o-t"h,-e-r-c:0:--:f:-;f,:-i-c"'i-a '"1 ""N""a,-m-e"")--
By 1/"-/
esp~:insible
AQ-15-6/23/71 Mailing
Oxforo, N. c. 27565
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0 . ; ·,.· NORTH CAROLINA DEPAR1MENT or tiA TUP.;L A:-◄J EC0:-1curc RESOURCES
Office of Water and Ai:-P.esoc:-ces
Air Quality Division
D P. Q. Box 27687
Raleigh, North Carolina 27611
E (Three Copies To Be Submitted}
(Fourth Copy Should Be Retained by Applicant)
APPLICATION FOR REGISTRATION OF PROCESSING OR MANU.FACTIJRING EQUIP..~E~if
I 1. o:mer of Installation Date of Application 00 t-JOT \'!RI 1 E I'' . ;',_.:;. ::: :-'-.·_::
Date Rec.· Reg. Date P.a-;. Sta:<:? T , .. , T r,T;-,i,.-n Vnit-c. 8-30-73 1:,ailing Address (P. o. or.St.) Telephone Acknowledgement:
I I rrlustrial Drive 693-6141 Date By:
City State Zip Code Reviewed By: Oxford, N. c. 27565 Name Date
Rea. I I I 2 .. Applicant or Authorized Agent Telephorye st;i tel I
Application Ret. to Ap.plica~t: ~· r,._ ... _ .... -----/t'aT!ing-Aoat~sS .... ..,....,,.. City State Zip Code Date By: I s cl me Registration Number: 3. Location of Plant Operation City. State Zip Code .
I rrlus trial Dr. Oxford, N. C. 27565 R-
I 4. Installer or Contractor (If Ne'N ".lr Replacement) Telephone Coordinates
. /_,tailing Address ~ity State Zip Code Class I .
5. Date Construction is to Start: Completion Date: . Date Existing Installation Placed in
.. .. Qperation:1L l 1966 I . 1c ;, ) 1 'l /fJ 6. Signature of Ovmer or Authorized Company Official Title Print or Type Name Title
Jim Patterson, Plant En·gineer I 7. Type of Registration (Check Qne)
Existing Installation-------~ New Installation-------------O Replacement------0 Fi 1'tera tion--------0
I Addition--------------------□ Change of Ownership----------□ Other------------0
Specify
8. 1.:ajor Ac ti.vi ty at this Location (Food, Lumber or wood Products, Primary Metals, Printir,g, Paper, etc. J
I Enittin'], Dy:ein'], Finishing Sic. No. Specify .
9. Total Number of Employees at this Location (Check Range)
I Less Than 10----□ 10-19-----------□ 20-49-----------0 50-99----------------□
100-21,9---------Eg 250-499--.--------□ 500-999----------□ 1,000 or More-----------0
I 10. Total Days Installation Being Registered is Normally Operated l□A• NUmber of Shifts
Days Per Week 6 Days Per Year 312 Shifts Per Day 3
I 11. Type of Installation Being Registered: (Examples: Kiln, Cement, Lime or Cal ciner) ; llA .. Number of Identica.1 Units (Tank: Galvanizing, Dip, etc.) (Furnace: Cupola, Crucible, Electric Induction, etc.)
1 'I1el1ter Frame # 1
Tenter Frame ~F 2 11B. Location in Plant I Dye Plant n 1 -f -..... ,... . I e, Specify II. J j' f ' 1 ,. t."-n .. , '· • 'A ; n1, I .Q-4
,·-· , ..
6/30/71 --..... • I a iv o',__J)J JJ -1-
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12. ~rindpal Materials and Quantities Used or Consumed in the Installatior. Sei.:-:g Registered:
Principal !,laterials
Nvlon l\cetate
Process W~ight (LOs./Hr.)
---------~Lbs./Hr.
---------~Lbs./Hr.
--------~Lbs./flr.
20.800.0QQ T '.? .-.
13. Principal Products and Quantities P~oduccd by the lnstallation Being Registered:
Princ~pal Products Quantity Year Uni ts o i P:tc-:=u.:tic:-:
Acetate 20,800,000 Yds.
14. Stack Inforr..ation for Installation Being Registered:
Height Above Ground Level (Check Appl'opriatc Height Ran"ge)
r:ot Applicable------:-.--0
100-149 feet----------0
Less than 30 feet---------[g] 30~49 feet------,-~~~ O .
200-249 feet-------~O
50-9?. f:et--~~~-~---=~-~~-[J
250 feet or More-------O 150-199 feet--------------0
Inside Diameter at Top, __ .11J2'---~x,.___J_u2:.___ __ Inches. Exit Ter.iperature,_...[[uD.1Lk~ ___ °F, Gas Ve loci ty ________ FL/1.Hn.
Stack Use: Fuel Combustion Products--------fI] Process Emissions---------~ Combined Use---------O
Ne;uest Builc!ing or Obstruction B!:yond Property Line (Exarr.ple: Trees, BriJgcs, etc,)
Type Cbs true ti on, __ _::'Ice' rc..:,e::.e=-:Sc:_ ___ _ Dis tan c Q, _ __::2::.:c:O..:Oc:_ __ ~_ foe t Height. ___ 4~0 _____ feet Di rec tio n._~E~· -~-'
15. Stuck Emissio:.s Control Equipment on this Instilllation ONLY \'/hen Gas Cleaning Device is Utilized1 "Supplemental Date Sheet
For Gas Cleaning E'quipr'.'!en t" Form AQ-5 · must accompany this Application:
Gas Cleaning Device: Yes--------0 No---------=E] Type. _____________________________ __,
Specify
16. Type of Fuel Used (Process Use 0:-ily -Do !'.ot Include Fuels Used for Indirect Healing:
Co ill Tons/Yr. Percent Sul fur % Percent Ash, ___ _
Oil __________ _ Gallons/Yr. Percent Sul fur % Grade Ho. ___________ _
Natural Gas, __ .:_X,_' ___ _ cu. Ft./YL L.P. Gas Other _________________ _
Wood,_~---------T0ns/{r. j) 2 Specify Kind and Arr-0unt
1,500,000 BTU/HR
j} 1 2,000,000 BTU/HR
17. Orgc.nic Solvents Used or Produced in this Installation Only:
Ara Oqanic Solvents Used? Yes-----O Mo------[3 Arc Organic Solvents Pr::,duced? Yes-------O No-------~
Q:.ianti ty Per Day (Gallons)
Speci fv hoe PrincioJl Use Consu:r.ed Produced
AQ-4 6 30 71
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0 18, Er.:iss1cns Fro!:': ihis lnstali~t1on Q:-ily_:
Polll:~ant (Spec: !'f "Type)
Exc:.,p!>?: H~S, S02, Cl2
!-:''/drocc.rbons, Dust, Etc.
Visible Emissions
A.dual Emissions
(With Existing Controls)
_____________ Lbs./Hr.
-----------~Lbo./Hr,
_____________ Lbs./Hr.
_____________ Lbs.jHr.
_____________ Lbs./Hr.
All Qu~~tities Should Be Deterr:iincd at.Maximum Production or Capacity.
Potential Emissions
(Without Control)
_____________ .Lbs./Hr."
_____________ Lbs./Hr,
_____________ Lbs./Hr,
------------~Lbs.'/Hr.
_____________ Lbs./fir.
19. Give Detailed Description of This Installation.
Include all raw materials, procc'Ssing equipment or machinery, chemical fore.ulas. Mhen applicable, and finished product
including any intermediate products which may be formed.)
Shoi,1 all quantities under Items 12, 13 and 16. Also, show fhwdiagram when it will clarify the process ot method of
pro due tion.
The equipment consist of a·gas fired oven for drying and ·heat setting nylon
and acetate fabrics. The exhaust system on· these ·uni ts are used fo·r the
removal of moisture out of.the fabric. Listedbelow·are the dyes and
chemicals used in our operations:
DYES: Disperse
Acids
Basics
CHEMICALS: Sodium Carbonate
TSPP -Tetrasodium Pyprophosphate
MSP -Monosodium Phosphate
Ammonium Sulfate
EDP TA Sequestrene cpd.
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F. Neal Hill NORTH CAROLI NA
APPLICATION FOR APPROVAL OF
PLANS ANO ISSUANCE OF
A "PERMIT"
TO CONSTRUCT ANO OPERATE AIR
POLLUTION ABATEMENT FACILITIES ANO/OR EMISSION SOURCES
Filed By: I.M. I. Warp Knits (NC) Inc.
(Name)
Industry Drive
(Address)
Oxford; N. C.
AQ-22 Rev. 8/72
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To:
NORTH CAROLI NA
BOARO OF WATER ANO AIR RESOURCES
Raleigh
APPLICATION FOR A "PERMIT"
To Construct and Operate Air Pollution Abatement Facilities and/or Emission Sources
Three Copies ~e Submitted
Board of Water and Air Resources
P. 0. Box 27687
Fourth Copy Should rcenlitj~;, . . J
Oate: 4/G/74 /:1 ',f) Co Raleigh, North Carolina 27611 J JI j li ·. ,n I
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, aJi)Jln
'is hereby made by I.M._I. Warp Knits (NC)' Inc.
(Name of Company, Establishment, Town, Etc.) (Include Division or Plant Name in Addition to Parent
in the County of Granville at Industry Drive, Oxford, N. C.
""co"'m_p_an~y~i'f'A~p~p~1,""·c-a~bl~e~) {Street and City or Town Address of Plant or Facility)
for issuance of a "Pennit" to construct and operate air pollution abatement facilities and/or emissions sources at above
location as specified in the accompanying drawings·, specifications, and other pertinent data:.
l. Nature of Operation Conducted at the Above 'Facility: Textile knitting, dyeing & finishing
2. Description of Process(es) Whose Emission{s) is/are to be Controlled by the Facility or Source{s) Which is/are to be
Constructed or Altered. (Complete Section I)
J
Textile tenter frame No. 1
3. Furnish Type and Narrative Description of Proposed Control Device{s).(Complete Appropriate Supplemental Data Sheets for
Control Device to be Installed and/or Operated. Include Make and Model Number of Control Device(s) and Number of
Identical Units).
Packed filter bed, high efficiency, medium pressure drop, oil mist collector.
Speizman Industries, Inc., Model 6-9 Poly-Maze Mist Eliminator.
4. Contaminant
Emitted:
Oil Mist
Weight Rate of Emissions {lb/hr):
Without Control Device With Control Device
14.1 < .71
Control Efficiency (%):
Without Control Device With Control Device
-0-> 95. 0%
5. Name and Address of Engineering Firm that Prepared Plans: Ross Engineering Associates
908 South Kings Drive, Charlotte N. C. 6. Ultimate Disposition of Collected Pollutants: 7. Dite on Which Facilities are to be Completed and in Operation:
8. Indicate Period of Time for Whi.z1JFacilities
are Estimated to be Adequate: __ ve·ars
_N_o_v~e_m_b_e_r_3_0 ___ , 19~
9. Estimate Cost of Air Pollution Control Device $15,000.00
Name: C._/ O'{;lf Y"7NT Mailing Addres_s:
(Responsible Individuaiif tompanyPurchasing/
I.M.I, Warp Knits (NC} Inc.
Operating Facility ... PLEASE PRINT) Industry Drive
Oxford, N. C. 27565
"""""'"""""" o.(/iR}/rvi ff« J(f: ''"""°"' "'"" 9'9 /693-6'4'
AQ-22 Rev. 8/72
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I. GENERAL DATA FOR PROCESSES
"'Wa.c.h deta.J.i.e.d pttoc.eA.b e.ng..itte.e/Ung dJt.aw.),ngA, e.qu..i.p-nent dlulwing.6 a.rtd 6low d..utgltllm6 601t the p,'LO·c.uA(e..6) OIL AouJtc.e.(.!i}
being c.oMbwcte.d 0:1. a.1:tVt.ed.
Name of Process: Tenter Frame No. 1
Total Weight of Materials Entering this Process: ~3_2~0_0 __ lb/hr or ton/hr nylon/acetate cloth
Volume and Temperature of Air Flow Entering Control Device: 14925
Volume and Temperature of Effluent at Discharge Point to Atmosphere:
Pollutant(s) tc be Controlled: Oil Mist & Flue Gas
Height of Process Stack or Vent Above Ground Level 25 ft.
Particulate Emission Rate {Before Control) __ 1_4_._l ____ lb/hr
CFM@ 337 .6 °F 10419 CFM @ 100
Inside area of Staclg J 3 2 ft2.
Particle Size Distribution: 0-Sp~. 5-l0p2-J;, l0-20p____i:, 20-30p____i:, 30-40p____i:, 40-50p____i:,>50~____i:
Gaseous Emission(s}: Name (Chemical Formula) or lb/hr
II. SUPPLEMENTARY DATA FOR INCINERATORS
Circle Type of Waste or Indicate Composition: Type 0 Type I Type II Type III Type IV
Combustible: ___ % Non-Combustible: ___ % Moisture: ___ % Heat Value: ___ BTU/lb
Total Waste Generated Per Day: ___ lb. Hours Incinerator will be Operated: ____ hrs/day
Design Capacity for Above Waste: ____ lbs/hr Manufacturer and Model Number; Approximate Cost:
Primary Chamber Volume: ___ ft.3 Secondary Chamber Volume: ft.3
Air Requirements: Total Excess Air % Draft: Natural Induced Other
Overfire Air: cfm Underfire Air: cfm
Flame Port Temperature: ---. Secondary Chamber Temperature: °F
Stack: Inside Area __ ft.2 Height __ ft. Gas Velocity __ ft/sec Temperature °F Fan Capacity __ cfm Stack lined? __ _
Is there a Wet Scrubber?
Yes No Flow Ra.te of H20 into Scrubber ___:_gal/min Temperature Before Scrubber °F
Aux. Fuel: Oil Gas Other
Primary Burner: Is there a Preheat Timer? Yes
Burner Rating: Primary Chamber
____ .BTU/hr
No Prehea~ing Time:
Secondary Chamber
----~BTU/hr
---~min.
Stack
__ BTU/hr
·secondary Burner or Afterburner: Is there a Timer? Yes No Length of Time Burner is Operated ___ min.
Is the Timer Reset by Charging Door? Yes No Other Mode of Burner Control
Type of Feed: Manual Automatic If Automatic, Describe
Signature:
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111. SUPPLEMENTARY DATA FDR FUEL BURNING SOURCES
•A.tt.ac.Ji. de.tailed. d,())1e,t6,i,oned dlw.w.<:ng ott .&ke.tch .&liow..ing -trite.1L1utl 6ea.tu,'le,& 06 _dftyeJW, woad 011. c.oai. 6-Ul.ed boileJU,, and
!f.CCOVVllj boil.e.,'1.~.
Type of Fuel Burning Source Tenter Frame Ill
Make and Model Number McCreary 19211
Stack Height Above Ground Level -1..5.._ ft.
Volume of Furnace ft3
Inside Area of Stacks.1.3...2ft2
II Specify Actual Alnoun t of Each Fue 1 Used in Above Source ( s) :
Coal lb/hr; Oil Grade __ Amount __ gal/hr, at __ BTU/gal and __ lb/gal or lb/hr
Wood lb/hr; Natural Gas 6000 SCF/hr, atl040 BTU/SCF; Other __________________ _
(Specify type, amount and heating value)
I Specify Maximum Rating for Each Fuel Burning Source:
Coal Oil Wood
I Maximum Sulfur Content of Fuel
Type of Solid Fuel Burning Equipment Used: Hand Fired Spreader Stoker Underfeed Stoker Chain Grate
I Stoker Fired with Ash Reinjection Traveling Grate_ Pulverizer_ Cyclone Furnace_ Other (Specify) ______ _
Ash Content of Fuel: Specify Method and Schedule of Tube Cleaning, if Applicable:
I Coal % Wood %, Other Lancing _____ _ Tube Blowing ______ Schedule ______ _
Emission Control Equipment {Describe in Detail in Sections IV and V)
I Collection Device: Wet Dry X Steam Injection Air Injection
Total Number of Fuel Burning Sources Within Property Boundaries:
I Maximum Capacity Rating, by Type, for A)l Fuel Burning Units Excluding that Itemized Above: (Total Like Units)
Coal lb/hr Wood lb/hr Oil gal/hr Natural Gas SCF/hr
I IV. SUPPLEMENTARY DATA FOR WET COLLECTION DEVICES
*A.tt.a.c.h dc.t.a.<le.d vig..i.ne.e/Ung d,'law{.ng.6 06 the. c.01itJt.ot de.v{.c.e. a.nd palt,U.c.te. .6-i.ze. veMu..6 1temava.t e.65,<.ci.e.nc.lj CU/LvU..
I Liquid Scrubb.ing Medium and Additives:
Total Liquid Injection Rate {Include ReCirculated and Make-up Rates) __ gal/min or gal/1OOO ft3
I Operating Pressure Drop Across Device __ in H2O
I ANSWER FOLLOWING QUESTIONS FOR SPECIFIC DEVICE:
VENTURI SCURBBER: Inlet Area in2 Throat Area in2 Thro.at Velocity ft/sec
GRAVITY SPRAY CHAMBER: Number of Nozzles Liquid Droplet Size u Co-Current Countercurrent
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WET CYCLONE:
Body Diameter in Length in
Inlet Area ---in2 Number of Nozzles
Outlet Ai--ea in2
PACKED TOWER OR PLATE TOWER:
Cross-Sec ti ona l Area ----ccc""7" ft2 Typ{<if _P,l_at_e,, ~
(
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Length \j . = >, 1\ !_·.: f.·i ~,.;;-Dept~ <,f '.E,i:kJTI e~r,ic \ii-. ~·:-ec·.ilaciai-·-JI~-·~ ·, VType:; Packi~g ____ _
I OTHER WET COLLECTION DEVICES: GIVE COMPLETE DESCRIPTION INCLUDING DESIGN PARAMETERS AND DETAILED ENGINEERING DRAWINGS.
I
Title: VP
D V. SUPPLEMENTARY DATA FOR ORY COLLECTION DEVICES
'A.t.ta.c.h de..:ti:u.,.ted e.ng-lne.eJt...i.ng CVl.aw.i.119-0 06 the. c.orLtlr.ot de.vi..c.e. a.nd pM-ti.c.te. 6ize Ve/l.6u.6 Jte.mova.l e.66-<.cie.nc.y c.Wtvu.
BAGHOUSES: Cloth Area ____ ft2 Bag Material
Number of Compartments ______ _ Pressure -Drop Total ________ in H20
Method of Cleaning ________ _ Air-to-Cloth Ratio------~--ft/min
Time Between Cleaning mi ns, hrs
ELECTROSTATIC PRECIPITATORS:
GENERAL:
Effective Area of Grounded Collector Plates ft2
Number of Compartments or Chambers ___ _ Number of Ce_l ls per Crimpartment _____ _
Electrical Field Gradient at the Discha.rge or Emitting Electrodes _____ KV/in
Average Electrical Field Gradient at the the Grounded Collecting Electrodes ____ KV/in
Fields of Treatment ____ Potential Applied to Emitting Wires ____ KV
SINGLE STAGE TYPE:
I Distance Between Emitting Wires and Collecting Plates _____ in.
Number of Isolatable Bus Sections ____ _ Corona Power ___ _ Watts/1000 cfm ·
I TWO STAGE TYPE:
Distance Between First Stage Emitting Electrodes and Field Receiver Electrodes {Ground) ____ in•
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Potential Applied·to Second Stage Emitting Plates ____ KV
Distance Between Second Stage Emitting Plates and Grounded Collection Plates ____ in
CYCLONES/MULTICYCLONES:
I Simple Cyclone
Diameter __________ in
Multicyclone
Diameter _________ in
I Inlet Dimensions ______ _
Outlet Dimensions ______ _
Inlet Dimensions of Individual Cyclone _____ _
Outl.et Dimensions of Individual Cyclone -----
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Pressure Drop _______ in H20
Number of Cyclones ______ _
Pressure Drop ________ in H20
Number of Cyclones _____ _
I OTHER ORY COLLECTION DEVICES: GIVE COMPLETE DETAILED ENGINEERING DESCRIPTION ANO DRAWINGS. (see attached)
Signature: _________________ _ Title:
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SPEIZMAN INDUSTRIES, INC.
POLY-MAZE MIST ELIMINATOR FDR THE TEXTILE INIX.JSTRY
I. PRINCIPLE
The POLY-MAZE MIST ELIMINATOR is designed to remove and =llect both liquid and
solid particulate fran a gas stream. Basically, the gas stream is passed through
a bed of packed fiber glass, with .the fiber micron size and the bed density deter-
mined by the characteristics of the ccntaminants •. The liquid particulate is collected
by the POLY-MAZE bed and gravity drains to the bottan of the system. Solid particu~
late is carried by the draining liquids to the =llection system. Provision is
made, however, for supplenentary irrigation of the fiber glass bed, if the liquid
draining is not sufficient to rerrove the solid particulate with nonnal liquid fla,,
rates.
The POLY-MAZE MIST ELIMINATOR utilizes Brownian mvement of small particles to
achieve the high =llection efficiency of submi=on particulate. Particles above
3 mi=n in size are =llected primarily by intertial impaction. The Br=nian
rroverrent becares increasingly rrore important in particle collection as the particle
decreases in size. The smaller the particle, the greater the Br=nian moverrent, and,
therefore, the higher the =llection efficiency.
An important part of collection efficiency is related to residence t:im;, of the
gas in the fiber glass bed. For this reason, the POLY-MAZE system utilizes a
design flow rate of approximately 25 FPM through the packed bed. The selection of
this la,, fla,, rate provides the folla,,ing:
Collection efficiency in excess of 95%
Long filter life because of la,, carq:,action pressures
L= pa,,er consumption, since the system will operate in the range of 5"
WG pressure drop.
II. DESCRIPTION OF THE POLY-MAZE SYSTEM FDR TEXTILE PROCESSING
The POLY-MAZE system involves three steps:
1. Filtration of Coarse Particulate
2. Cooling of the Gas Stream with a Heat Reclamation System
3. Collection and Rerroval of the Particulate
Central Fi\e Cop~
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1. · FILTRATIOO OF COARSE PARI'ICUIATE
The gas stream is exhausted fron the tenter frame at approximately 300°F.
The hot gas stream is passed through a grease filter at roof level to rerrove large
liquid droplets, lint, and other coarse particulate. The collected liquids drain ·
to a holding basin. belew. The filters can be renoved for cleaning. Hewever, a
steam line is provided at the filter location, so that they can be cleaned in
place.
2. . COOLING THE GAS STREAM WITH A HEAT RECLAMATION SYSTEM .
It is important that the gas stream be cooled to approximately _100°F. before
it reaches the POLY-MAZE filters. The contaminants in the gas stream are primarily
in a gaseous state above 160°F., and the cool-d=n cycle is necessary to assist
in the condensation of these hydrocarbons. By lewering the gas stream temperature
further to 100°F., the particulate develops a physical ·state that enhances the life
of the filter beds.
The cool d=n involves passing the hot gas stream through a water coil heat
reclamation system that cools the gas stream frcm 300°F. to 100°F.; further, the
heat reclamation system provides hot water that can be used in the dyeing operation.
3. COLLECTION AND REMOVAL OF THE PARI'IClJLATE
The cooled gas stream new flews to the inside of the POLY-MAZE filter
chamber. The finer condensed materials pass through the filter beds, coalesce
during residence in the filter rredia, and drain through collection pipes to the
holding tank on the bottom of the housing. The larger particulate that collects
by inertial impaction drains frcm the inner surface of the filter bed to the
holding tank belew. The collected materials are periodically rerroved by a waste
disposal service. The clean filtered air is exhausted to the atrrosphere.
III. DESCRIPTION & SPECIFICATIONS OF THE POLY-MAZE MIST ELIMINATOR EQUIPMENT
The POLY-MAZE MIST ELIMINATOR is manufactured by Speizrran Industries of Charlotte,
North Carolina. The system being offered is Model 6-9~ which is supplied with six
fiber glass filters, each with a filter.area of 60 ft. , and a total filter area
of 360 ft. 2 • The total SCFM presently being exhausted from the tenter frame is
9918. Under present operating conditions, the flew velocity at standard conditions
through the filters is 27.6 FPM.
The fiber glass used in the filters is a special filter rredia continuous-strand _
rreterial supplied by PPG Industries. The fiber glass beds are manufactured by
Speizrran Industries frcm the material supplied by PPG.
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The POLY-MAZE filters are equipped with an intemal spray system to be used only
if the filter media becares flcxrled or clogged. This condition can te deteDTri.ned
by observing a significant rise in pressure drop in the system. A pressure gauge,
. which is rrounted at a convenient location, is supplied with the equiµrent. Wann,
detergent water would be used to flush and rinse the filters until nounal operating
conditions (pressure drop) are restored. It is possible for the system to remain
in operation during the irrigation of the filters. If, ha,,,ever, the system has
to be turned off during internal inspection, intensive cleaning, or for other
· naintenance reasons, it would becare necessary to shut da,,,n the tenter frame to
prevent the loss of air contaminants to the open air.
Central File Copy
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VI. AREA DIAGRAM
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CMner I.H.I. Warp Knits (NC) Inc.
Locationindustry Drive, .Oxford, N. C,
(Give Street Address)
INSTRUCTIONS:
1. Show all surrounding buildings and roads within
1000 feet of subject equipment which is located
at center of circles.
2. Inaicate location and type of building by the
use of small numbered circles with the de-
scription below.
3. Show roads as lines representirig the road edges.
Indicate street names and highway numbers.
4. Show wooded or cleared areas by approximate
boundary lines and the words "woods", 11cleared11 ,
"cornfield" 1 etc.
5. Indicate direction of north by arrow.
DESCRIPTION
(j) I.H.I. Warp Knits
® Office
G) ffoiler Room
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EXAMPLE (j) Church
® Residence
X Indicates location of equipment.
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OUI'LINE SPEJ:IFICATION
FOR
HE'AT REO)VERY A..'ID
AIR POLimION CONTRJL SYSTEM
FOR TENI'ER FRAME NO. 1
I.M.I. WARP KNITS (NC), INC.
OXFORD, N. C.
ross ENGINEERING ASSOCIATES
FOR
HILL ENVIRCNMENTAL GIDJP
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01-GENERAL:
Contractor shall provide a canplete and operable heat recove:ry and air
pollution control system for tenter frarre no. 1 at the I.M.I. Warp Knits (NC} Inc. Plant in Oxford, N. C. as herein described and as shown on Ross Engineering
Drawings M-1 thru M-2.
Heat recove:r:y and air pollution control system shall be canplete with all necessa:r:y fans, 110tors, starters, drives, ductwork, dampers, coils, filters, housings,
insulation, pumps, piping, tanks, mist eliminators, controls, valves, wiring,
supports, and accessories as nay be required for a canplete and operable system.
Sys.tern shall be designed to recover heat from the tenter frarre exhaust stacks and gas burner flue gas stacks and to use such recovered heat to heat water which
can be stored in a hot water storage tank and subsequently be used as supply water in the dyeing operation; and to re=ve particulate natter from the _exhaust stacks and flue gas stacks and reduce the emissions from such stacks to. a level which
will be in accordance with the requirerrents of the Air Qualit:y Division of the
Office of Water and Air Resources of the North Carolina Departrrent of Natural
and Econanic Resources.
02. DESCRIPI'ION OF SYSTEM:
E..~.haust gases fran tenter frarre no. 1 exhaust stacks and gas burner flue gas stacks (consisting of hot, 110ist air, oil mist, and products of cc:rnbustion}
shall be conveyed by a system of sheetrretal ductwork (which shall tie into the
existing tenter frarre exhaust and gas burner stacks above the roof), through a
double set of lav efficiency filters, a water coil (which shall cool the air stream and heat water}, a fan, an air _pollution control device, and thence to the atrros-
phere.
The water coil shall be supplied with a constant quantit:y of pumped water which shall be heated by the hot air stream. and delivered to a storage tank. The water delivered to the coil shall be a mixture of storage tank water and unheated raw water as nay be required to rraintain a rraximum air temperature supplied to the air pollution device, maximtnn and minimum water temperatures delivered to the
storage tank, and a minimtnn storage tank quantit:y. The hot water _in the storage tank shall be pumped to the existing dyeing area where it shall be nade available
for use at each piece of _dyeing equiprent;
The air pollution control device shall re=ve particulate oil mist from the cooled air stream before the air is exhausted to the atllOsphere. Air pollution control device shall remove sufficient quantit:y of particulate natter to insure that
emissions fran the exhaust of the device shall confonn to the air pollution control standards as set forth in Regulation No. 2, Section II; Enission Control Standard
2.30, Section IV; and other such applicable sections of the "Regulations Governing
the Control of Air Pollution" as adopted by the Board of Water and Air Resources.
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All liquid oil collected from the lcw efficiency filters, water coil, fan, ductwork, and air pollution control device shall be conveyed to a central oil
collection station for disposal.
. 03. EQUIPMENT SPECIFICATIONS:
A. Ductwork:
All ductwork shall be rectangular or round sheetmetal ductwork fabricated
of galvanized sheet steel in ac=dance with the Sheet Metal and Air Conditioning
Contractors National Association, Inc. "High Velocity Duct Construction Standards"
and Industrial Ventilation Manual, Section 8, "Construction Specifications for
Local Exhaust Systems" Class I Duct.
All ductwork shall be sealed to prevent air· leakage, properly re-inforced, supported and·braced for structural strength, and sloped _to facilitate
oil collection, and with necessary darrpers and regulators.
B. Housings:
All housings shall be fabricated of galvanized sheet steel or painted
black sheet steel in accordance with the Sheet Metal and Air Conditioning Contractors
National Association, Inc., "High Velocity Duct Construction Standards". Housings shall be ccnplete with all necessary access doors, drains, reinforcing, etc.
c. La,, Efficiency Filters:
Filters shall be permanent, viscous type, unit style, with rretal fr=s and riietal rresh rredia, and shall be designed to operate at a temperature of 350° F.
Filters shall be rated at an A.F .I. efficiency of not less than 60% at 450 PPM
face velocity, a final resistance of .50" W.G., and a minimum dust holding
capacity of 480 grams. Filters shall be installed in two banks with side access.
Filters shall be enclosed in a housing with provisions for cleaning and rerroval of
collected oil.
D. Water Coil:
Water coil shall be extended surface, staggered tube, plate fin type
with 5/8" O.D. seamless copper tubes, seamless copper tube headers, rippled aluminum
plate fins, and galvanized steel casing. Coil shall be designed to cool 9918 SCFM of air from 337.6° F. to 100.0° F. while heating 40.0 GPM of water from 50° F. to 177° F. Coil face velocity shall not be greater than 425 PPM with an air side resistance of not greater than .50" W.G. and a water side pressure drop of not
greater than 5.0 feet. Coil shall be enclosed in housing with provisions for cleaning and removal of collected oil.
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E. Fan:
Fan shall be a single width, single inlet, backwardly inclined, non-·
. overloading airfoil blade fan, ccmplete with =tor, v-belt drive, manual _inlet damper,
access door. Fan shall be arrangerrent No. 9, clockwise rotation, bottan horizontal
discharge,. Class Il construction. Fan shall be designed to deliver 10479 CFM at
100.0° F. (9918 SCFM) at 9.0" S.P. Brake horsepa-ler at design conditions shall
not exceed 20.0 horseJ?Gler and outlet velocity shall be less than 2600 FPM.
F. Air Pollution Control Unit:
Air pollution control unit shall be a l= pressure drop, high efficiency,
packed bed oil mist collector ccmplete with packed fiber9iass filters, internal spray
system, holding tank, heavy duty steel housing, pump, drain, pressure gauge, and
accessories. Unit shall be designed to handle 9918 SCFM at a temperature of 100°F.
with a pressure drop of not greater than 6.0" W.G. Velocity through filter ll'edia_
shall not exceed 30 FPM. Unit shall be designed to re110ve 99.9% by weight of all
· particles 3 microns in size and larger and 95. 0% by weight of all particles less
than 3 microns in size. Unit shall be a Speizman Industries, Inc. M::ldel 6-9 Poly-
-Maze Mist Eliminator or approved alternate. During nonnal operation the emissions
from unit stack shall contain not l!Ore than .71 lb./hr. of particulate based upon
an entering rate of 14.1 lb./hr. and the density of the emissions shall not exceed
that as designated as No. 1 on the Ringelmann chart.
G. Water Storage Tank:
Water storage tank shall be a heavy gauge black steel, vertical water
storage tank with phenolic lining. Tank shall have a capacity of not less than
24,000 gallons. Tank shall be =nplete .with fittings, manhole, vent, and accessories.
Tank shall be insulated with l" thick glass fiber insulation with rib almnim.nn sheet
facing. Tank shall be Il'Ounted on ccncrete pad.
H. Punps:
Pumps shall be_frame Il'Ounted, end suction, centrifugal pumps ccmplete
with =tor and base. Recirculating water pump shall be designed to deliver 40 GPM
@ 30 foot head with 3/4 HP =tor. Pump for dyehouse supply shall be designed to
deliver 120 GPM at 100 foot head with 7-1/2 HP Il'Otor.
I. Piping:
Hot water piping shall be black steel pipe with screwed fittings. Pipe
shall be insulated with l" thick glass fiber insulation with canvas jacket.
Copy
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J. Controls:
Contractor shall provide a system of controls which shall
provide for autanatic control of the heat re=very and air pollution control
system. Supply temperature of water delivered to the water =il shall be con-
trolled by leaving. air temperature. Control shall also maintain minimum water
level in tank. Recirculating pump shall be on any time the air pollution
control device is in operation. Hot water delivery pump shall be controlled
by hydro-pneumatic tank which shall bring pump on anytirre hot water is required.
Control shall also maintain minimum water level in tank.
K. Guarantees & Test:
Contractor shall guarantee all equipment, materials, and work-
manship for a period of one year £ran date of final acceptance. Contractor
(through the air pollution =ntrol device manufacturer) shall guarantee the
performance of the air pollution =ntrol devire in ac=rdance with the require-
rrents of the Board of Water and Air Resources as previously specified. Indepen-
dent performance tests will be made by Hill Environrrental Group to detennine
actual field installed performance of the equiprrent, and in the event that the
performance is not the standards required by these specifications, the Contractor
. shall make such corrections, adjustrrents, replacerrents, etc., as may be required
to obtain the required performance.
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NORTH CAROLINA DEPARTMENT OF WATER AND AIR RESOURCES
AIR QUALITY DIVISION
REQUEST FOR ACTION TO BE TAKEN __ .
/J I· '._._ ~_ ~. ' :: ,. : . ""·
,, 1:... . •, ... ' -.• The item listed below requires action to ascertain 'compliance under Article 21, _Chapter 143 of the
General Statutes of North Carolina, concerning rule~.,_,arid' r'egul~tions · governing the ·control of air: pollu-tion : ·· · · -~ '~ •~ f' j
Name Address I. M. I. t'/a:-p Kni-::a, O;cford, :-ic,rth Carolina,
Subject
AQ-22 for mist eliminator on tenter frame No. 1
Investigation Requested By · c. J, :'.l'll::-ya;it
Remarks
conduct review and make recor.unendation!j
Assigned To
Eng. Bra.1ch/[.fnrshal. l Rac~<ley
IJlvestigated By
Derr Loonhai·d.:
Action Recommended
Investigation Report
Address
Ox£or<I, ~!or-::h Carolina,
Date "/.,/''' :., ' ..•
County Granville
County Granville
Date
4/24/74
Retllrned
5/3/74
2. J~ie2:1J.;1 r1.1cb]d. b.:::d oi.l :.ii.::r..; ~'.Jl!.ccto::: i5 1:0 U·~ i:1i.i·c.1il,3rL (:-iod·Jl (J-9 ?uly .. ~Jaze) •
T!iis :.:qaip~;1ont is :.. r::wsll 1)1d ~,;..·p: ~:.i!.;'!: :;L~i.::.:li:~·t:Jl~.; ?.:ic.i.,:in;; is .ti~~rJrL1.ss. Six
illtc:.::.; i~l ~al".: l.!:l~~} ~-:it·;1 :]. 1:..1.t:::::: ~:·.-.!a ,-;:E 1:~o :)•~!-I:.:. :70i' a :::1t~?.l -J.f J(1i] sq. ft~
.-\-.;: ~~l:ii3 ;;.:";·,, (:1-J.:..~.-a~.: a.i::·flv~;) -~~;o £~vw 1/;)l•Ji;ity l::; 27.6 f-t./::1L1. (0 ♦46 ft•/'Jcc.).;
"1'"c 1"";,,t ,.j-i•,a··1·1 ~·-~-A .... -.,••.:-..•1·,.,· ,•·-O, .. r-.-... ·1•• '"; ... ~,-~. r·.,~,r.· '1"1,r:1•0 t .,,_.,..c!1•1'c ... • "·1l'eti'n " 14)
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•~1·m1·-:.,~ -,~.;-ro c~j ..... -,..:-,~--o .. ilri"J'"".) '1:1·.r·l ;~ .. ,,.-; .. ·\1--,•·•~1 ... r.:-,,. .. ·i·J.·,,, . .!'I ....... 1•·-.,,, .. 11·11" v1·•1"ole ._, ............. ._ ... .,_. •--'••._,..,,_,., ._,, -•• ,..., • ,I I.,; J,.--.,.~ .)'.o. v... ..,..__•·•-..-w• ..._" ._,,J. 1,,.._uJ.. (,> W
emissions,. .:kt.-1s·-1 ~r, a3 J:C1a.Lut ~{~\s (::J i::-orn tla.i burner as w,:, 11 as the tenter frame
are to be. ·creat1.;:i, .1 visii)le e:n.issiu:1s evalwtion for compliance is reconLacnded~
AlloNo.lJl~ parti:;uJ.J.tJ ur;,lssiou:;, :ll"O :.i.~ H.l~e/h":.. ... (3200 ll>s•/hr~ _proce33 rate)~
Un:o~TtrollcU ~n::i:;s.i.011.:; .l.r-J appro;~, :;_,) l'..n;~/!1r. (li2rJ oil); ;·Jocessary efficiency
:for cora;,liarice is 65. 61J. Tl!i.s filter should a6ievc approx. 9,J:~ efficiency;
(P.ef. D,'BA-14).
Facility should eomply with applicable reguladons.
;·iegul::n;ion 8 does ao't apply.
RRO/Ron Hawks indicates that equipment proposed is acceptable under the terms
?f TP No, 2428,
Correspondence To:
White-Engineering Branch; Yellow-Central File; Blue-Regional Office; Green-Engineering Branch
AQ-16 Rev. 7-1-71
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Mr. c. J. o• Brya:1t
E:-~ecuti vc Vice FrcsiCent
, I.·M. I. i"/n:-p !~nits CiC) I:1c.
IE,..1.ust:ry Drive
Oxford_. !;o:-.th Carvli;1~ 27:~ti5
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Central
Su!.Jj cct: Pe_~r~i-~J:.}!?• ZQ,PJ ·-··►•• .. --, .. ,__
I~--:-l. I. Warp Knits (!~C), -r~H.:.
'----Oxfo:-d, ilorth _ C:irol_~i1:1_
I:i accorl!a:1ce·. i'iith yc11r aµplic::ition datcG i\1)ril 2-+, 1974, h'D are forH2:-,.i-
in!! hcro1'lith f-!.!r;siit :-Jo, :.:::J:J7 to I. :,1. I. Warp !G'lits C~CJ. Int:.._ 0.xfcrJ, >iorth
Carolin:-l, fur the coi~struction :i.nd-oper~tion of ~n ~ir clen:i.in.q. device cou-
sis~:.i·;~.r, of ..i fil)e::-r.~l:1s:; ::10si1 paJ trp0. ';:1.ist L!li:-:-.i:1-1.?:c":-(3t10 sq. feet of fuc~
:tl't.!al ;.?.r~c: a:.:p1.~r•:~!1:11~~cs 2.:1~r.ailcd. on tenter :f:-a::1e tJo. 1 to rm:-iov,.; r,;1rticulat.e
anJ ~isil:le· ~ni.ssior1s, a~1ri :::'o:r tilt! discl~Urge o:: tb.! t::teatcJ a.ir into ~he
t"'utdoor.at:Jos1ihcre ~n:. its facility loc:1t•.!J ,1t·-Iridu.s-::ry Driv0, Oxford, ,·~ort:1
Carolina, Granvil.lt.: Cr:unty.
Thi!i P!.;1·i:-,it sh.:-!.ll Ju effective frrn:1 tJ-:.c date o.f its issu.:u:icc tmtil Dccci':1D~r
31, 1977, J.nd sitall l.;~ subject to tht.!. ccnditim1s ~nid li:nit:~ti,;Jns ~ s~1ccifi!~d
therei:n.
'011c sc·t of t:-1:·! ·Pe~.1it. Applic:u:i,"Jn 1nd plans a~:11 spec.:Lfication~ is btii:1~
Tetun1cJ. to yon wi t;i L:is 1:..•ttc:r.
Eaclo!; urc.s
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m)Ai<D OF
For the DischarEe of ·Air ContamirlantS Into the Atmosphere
· In accordance wit!: the provisions of Article 21 of Chapter 143, General Statutes
of Xorth Carolina·aS amondc<l, ar:<l oth~r applicable, Laws, Rules arid Rei!Ulations,
,
Pt;t'.lISSION IS EEREl\Y GltA\Tt'D TO
r. M, r. Warp Knits ('<C), Inc.
Oxford,., l-ior-th Carolina
FOR TliE
cunst1"tlct.ion· and operation of nn air clc~uinr; d·evic~ cor.sisting of '.1 fibe-rglass
;aesh P<f<l type nist eliminator (360 sq. feet of face area) :rn<l a;,purtenanccs installed
or; tenter' frame l-~o. l to remove pa1~tictll:1tc and visible er.iissions, nnd for the -
<lischnr2:e o.f the treated -air -.into the outdoor atmos1Jherc a.t its' facility located nt.
1::Justry Drive, Oxford,· North Carolba, Granville County,
i:1 accor<lance with the -application. d:itcd April 24 1 1:174, and in conformity wi1:h
the plans~ specification$, and otht!r su?portinn dJ.t:i, all of which n.re filed \•Jitit
the Office of i':3tcr and Air R-·Jsources a.rid a~e considerc,d a part of t!:is P~r:r:it.
T:d!> P0rnit s!1:ill be _e?fcct'ivc from the lfo.tc of its issuan..:e until December
31, l'.lP, and 5hull be subject to the follo,:i1!g S'.)edfired ccnt!itio:-,s :mJ li::li,::rcicns:
1. This Pe:rciit sh3.ll bBcomc vciJ unless t!1~ facility is constructcJ in ac..::ordance
. with the approve,!' plans, S!1cci ficzitio~1s and other su;_)rorting tlata nnd is
complotc<l and placed in o~,oration on or before ~fov.cm!;er 30. 1974. or as this
date nay b~ a.-:i~i1.Jc.J.
2. · ·chl.!. ~ir clcani:13 <lcvic0 shall be prcpc-::.·ly_ cpc1·at,:.:J :it ail tim~s in such a
i:1anncr us to effect a:1 overall r~~<lu.ction in air. -:1oll1.1t.ion substantiall v in . . ,
kecpin~ wit!t the O.tll'lic:ition and ot:1erwisc to rctluc~ air ccntnminat:.m1 to the
extent necessary to crn;1;_)ly with applicable .rcgul~ti0ns anJ stn.ndn.r<ls.
:}. Reports on the operation n.n<l testiZ1.g of the f:.icility shall be 5td.:a:littc<l to
the ;:orth Carolina Qffic:3 of :VatLlr and Air Rcsou:-cc1; at 5ttd: intorvals and in
suc:1 for;:1 and detail as may b:1 required Uy the Board or its a.J.:1inistrativ~
staff.
-i. This Pcr1:iit is lssus..!t! with t!:c stl:n1l:1tion that thi~ facility will be evalu:ited
for-co:r.pfi~n!ce i.,.i. th a1.1plicahl:.~ re1;ulations by this Uf.fice, ut t!1c aforu:1c-ntior.cd
location;. within 90 ,fays of the operational date, This P,m:1it shall b,1com-,
voicl. with proper notice· to the c01:ipany, if the results o~-= t:1c evaluation
indicate that the facility <lacs net meet applica~ili:-l~ws, rul~s, a:11:.! rc_iJUl:ttions.
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:10!,T: ! CAIWLI,i.\ BOARD OF liATER ;\;·!!) Arn !!iSOuRCES
By ? ? ?~ / ,_ c.--1',--j_..-__..:::zP
E~-·c. l:u!i-b:2rJ. As::;istant Dircc\.or
Officf.!' of W:1.ter anJ .:\ir rrcsour~s
Central
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/J ,I ._J_}__(U ;t;J--v~L-OFFICE OF
f WATER AND AIR
North Carolina Department o REsouRcEs
Natural & Economic Resources ,.c. ~,~~~~~~
JAMES E. HOLSHOUSER, JR., GOVERNOR • JAMES E, HARRINGTON, SECRETARY
BOX 27687. RALEIGH 2761 l
TELEPHONE [phone]
~11:1-l'a,,,i;~., Plant Engineer
( I. M. 'I. WA.'U' KNIT!::,
~fiiil Drive~-
o~ford, North Carolina 27565
Dear Mr. Patterson:
June 20, 1974
Central File Copy
The North Carolina Office of Water and Air Resources, Air Quality Division
has completed review of your application for registration of the installation(s)
listed below, which are located at the following address:
Industrial Drive
Address
Oxford
City
Granv:;I 1 le 27565
County Zip Code
This is to inform you that this (these) installation(s) has (have) been
registered and has (have) been assigned registration number(s) shown below.
Registration alone does not imply that the installation(s) is (are) in
compliance with applicable emission control regulations; therefore, you should
ensure that such equipment is in compliance.
Thanking you for your cooperation, I am
Installation Registered
-Tenter Fram& Ill
Tenter Frame 112
Dye'l'lant
ames A. McColman, Chief
Air'Quality Divisiori ·
Registration Number
39-73-12-0019
39-73-12-0020
39-73-12-0021
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WILLIAM 0. ROSS. PE
ROSS ENGINEERING ASSOCIATES
908 SOUTH KINGS ORl\~E · CHARLOTTE, N. C,
Mr. Jim Patterson
I.M.I. Warp Knits {NC), Inc.
Industry Drive
Oxford, North Carolina .27565
Dear Jim:
November 18, 1974
28204
In accordance with your request we have reviewed the proposed air pollution
control and heat recovery system for ~enter frame No. l.
10.c,,1,.1a,2
The attached owning and operating cost analysis is based upon our conservative
view of the situation. Installed equipment costs have been figured on the high
side, while energy savings have been figured at current rates.
It would appear, from the results, that the heat recovery installation would be
self liquidating during a reasonable period, but could not be counted on to totally
amortize the air pollution control equipment. However, over the life of the instal-
lation it would give substantial credit toward the air pollution control equipment
cost.
The results are based upon installed costs of the systems, plus maintenance,
energy, and cost of money.
I have also based the calculations on not providing heat recovery from the flue
. gas stacks as the additional energy recovered would be difficult to use at the frame
and would often require that this energy be rejected to the outside air.
We are prepared, upon your instruction, to proceed to complete the drawings and
specifications and go out for bids within three to four week~ of notice to proceed.
Delivery of equipment would take six to eight weeks and an additional two weeks would
be required to complete the .installation. I suggest that we go out fo~ bids around
December 13 with bids received around December 30. This would give us an approxi-
mate start-up date of March 15, 1975.
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Mr; 'J'im Patterson
November 18, 1974
P·age 2
We look forward to hearing from you as to which direction we are to take at
this time.
cc: Hill Environmental Group·
WOR:bw
Sincerely,
ROSS ENGINEERING ASSOCIATES
-7; ~C://?o--vz_
William 0. Ross, P. E.
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:u
l.~.I. WARP KNIT• (NC) INC •.
INDUSTRY OR.
OXF0RD.N.C.27~65
TEL, 919-6Si13-15l41
November 24, 1974
NOV 25 1974
Mr. Brock Nicholson
Chief Engineer
Air-Quality Division
Civ. o; E:;v'rc::;;;~:,tcal Mat.
f~'.cf,:;h, N. C.
Deparbnent of Water & Air Resources
Raleigh, North Carolina 27611
Subject: Pennit No. 2097
Dear Sir:
Enclosed, please find a status report dated February 15, 1974
which was our original plan of action for instituting emission control
and a heat recovery system on the equiµnent in question.
Based upon the original schedule we were issued a Permit No. 2097
on or about May 15, 1974 and we proceeded to receive bids on the proposed
equiµnent.
On or about June 30, 1974 we reviewed the bids and the concept to
be utilized. At approximately the same time, we became aware of the
potential acute shortage of natural gas in North Carolina and decided
to investigate the possibility of reducing our gas consumption in
conjunction with the pollution control equiµnent, since we believe it is
in the best interest of the State and the company to do our part in
conserving natural gas. ·
At this time, we asked our consultants (Hill Enviromental Group &
Ross Engineering Assoc.) to initiate a feasibility study of the gas
consumption reduction concept.
We received the results of this study on November 24, 1974, therefore,
making our compliance date of November 30, 1974 impossible to obtain.
We, therefore, respectfully request an extension on our compliance
date based on the follc:Ming revised schedule received from our
consulting engineers (copy enclosed).
November 22, 1974
December 21, 1974
Begin Engineering drawings of
proposed system.
Spjciification~
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January 15, 1975
February 1, 1975
April 1, 1975
April 15, 1975
April 30, 1975
Receipt of bids.
Review bids and award control.
Delivery of equipment.
Installation of equipment complete.
Perfornance testing and final
acceptance.
Based on the above time table, we request an extension of our
compliance date to April 30, 1975.
Hopefully this. request will not be contrued as an attempt to
dodge our responsibilities, but will be recognized as a true effort,
on our part, to comply with State regulation and do our share in
conservation of our natural resources while utilizing sound business
economics.
JHS/mgo
cc: Hill Enviromental Group
Ross Engineering Assoc.
Jack H. tanley
Plant Manager
... \ 7
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Copy to Derr Leonhardt
NORTH CAROLINA DEPARTMENT OF WATER AND AIR RESOURCES
AIR QUALITY DIVISION
REQUEST FOR ACTION TO BE TAKEN
The item listed below. requires action to ascertain compliance under Article 21, Chapter 143 of the
General Statutes of North Carolina, concerning rules and regulations governing the control of air pollu-
tion:
Name Address
nu Wllll! Knits Oxford
Subject
Request for extension of installation date on Permit 02097
Investigution Requested By Address
.lk!xth_Gentral Region
Remarks
Temporary Permit issued for visible emissions and expired 11/30/74
. Assi;;ned To
North Central Region
i"rlvestigated By
_Melvin Flora
Action Recommended
accept request for extension
Investigation Report
Date
12/10/74
1. Contacted Mr. Jim Patterson, Plant Engineer,
County
Granville
County
Date
Returned
12/10/74
2. Discussed with Mr, Patterson the extension requested by his company received 11/25/74,
3, Il1I has shown good faith and this· representative recommends acceptance of extension
request, (sse letter received 11/25/74)
Correspondence To: ------------------------------------
Signature: __ '-],.,__-=--==----'--------------
White-Engfoeering Branch: Yellow-Central File; Blue-Regional Office; Green-Engineering Branch AQ-16 Rev. 7-1-71
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NORTH CAROLINA DEPARTMENT OF WATER AND AIR RESOURCES
AIR QUALITY DIVISION
. REQUEST FOR ACTION TO BE TAKEN
The item listed below. requires action to ascertain compliance under Article 21, Chapter 143 of the
General Statutes of North Carolina, concerning rules and regulations governing the control of air pollu-
tion:
Name
I, M, I. Warp Knits Inc.
Subject
Request for amendment to Permit No. 2097
Investigation Requested By
Jack Stanley
Remarks
Conduct :-rn;·ic.11 m:tl l.il.'1kc ::cc.cn:I"'.en<lu.tions
Assigned To
EnJinccring ~ranch/RlO
Iflvestigated By
D2rr Leobhardt
Action Recommended
Investigation Report
Address
Cr.:iurd
Address
0-,cford
Date
December 17, 1974
1. Pem:f.t. l\\,. 20?7 ha<l ,!! cornpletfor. -:!ete· of No,r~ber ~('), 197l1.
County
Granville
County
Granville
Date
aovein1>er·25, 1974
Returned
December 17 1974
2. I, M. I. Warp !/'nits wishes to delay this completion date until April 30, 1975.
3. The cea$On f-'.>r the d~lay is @,h·!!n r.e a desire to in.corporate a heat recovery system
as a part of the t!!ist eliminator proposed. The engineering of this system along
Trlth the lc:tti~ c,£ bi&$ for the !i!!<trs equiJ?rr.ent acco11nts for the delay.
4. This request appears reasonable. RRO/l'lors ccncurs.
5. The addecl equipment will not dccrea11e the efficiency of the equipment already prppose
I 6, I recammend that the Permit be so amentlad.
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Correspondence To:
White-Engineering Branch; Yellow-Central File;
AQ-16 Rev. 7-1-71 Blue-Regional. Office; Green-Engineering Branch ', ,i' .. ~,i :,{ ; ,i ";' ~; ·. .. ...
·J 'I . ,:,1 1 ... ·,;, .(_ .. _:i_ ·:. \.,, ·\-:'/ ,;! -' ·~ "
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NORTH CAROLINA DEPARTMENT OF WATER AND AIR RESOURCES
AIR QUALITY DIVISION
REQUEST FOR ACTION TO BE TAKEN
The item listed below requires action to ascertain compliance under Article 21, Chapter 143 of the
General Statutes of North Carolina, concerning rules and regulations governing the control of air pollu-
tion:
•.~Warp_)
Saliject
Address
Oxford
,..--~o.unty=====-...... ,..-.. . " , -. Granville ·
/ I Contract let duo Fobruary 1, 1975
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Investigation Requested By
North C
Remarks
Jim Patterson, Plant Engineer
. Assigned To
North Central Re~ion
i"rlvestigated By
Melvin Flora
Action Recommended
contact by end of February, 1975
Investigation Report
Address
Date
2/11 /75
1. Contacted Jim Patterson, PlantEngineer, .IMI Harp Kn:!.ts.
2. Contract liao not been let due to econooic reasons:
a, Capital expenditure for LP gas stand-by -approximately $100,000.
b, 50% reduction in production
County
Date
Returned
2iliii5
3, Hr. Patterson questioned the po3sibility of postponement of Environment regulations and
compliance schedule.until economy improves.
4. Regional personnel advised Mr. Patterson to present a firm status report by the end of
February,. 1975·, At that time, any requ,rnts for additional time should be made with
definite plans as a special consent order will probably be required.
5. The v~.olat:!.on in question is a:v:!.siblo emissions problem on tenter frames. Thia violati
fa somewhat reduced by the 50% out in production.
6. Extans:!.on of time has been granted once on their compliance schedule. The reason for th
first extension was to design a control device with a heat rec.:>Very system instead of a
control device with a single purpose.
Correspondence To:
Signature: 7,
White-Engineering Branch; Yellow-Central File; Blue-Regional Office; Green-Engineering Branch
AQ-16 Rev. 7-1-71
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. Mr.· Jack B. Stauley
1'lont Manager .
I. H; I. WARP KNITS (NC) . INC.
Industry Drive
O:sford, North Carolina 27565
· Dear Mr. Stanl.ey1
February l7, 1~75
Your letter dated Nqvembar 24, 1974 requests that the operation date contained
in Permit No. 2097 be amended to read A~r:!.l 30, 1975 tlue t~ the add:!.t:!.on of a
heat recovoey system to the control equipment. lt ie the opi1:.:!.~n. of thic Office
thst the r5quest. in valid and re!ll!onable,
.
Accordingly, the above referenced Permit is amended es follows:
The pbraoe " ••• placed in operation on or before November 30, 1974,
or as tbill date may be llllllilllded." i& changed to read ", •• placed in
operation on or before April 30, 1975, or as thid date may be amended,"
All other conditions and specifications of the original l'ermit No. 2097
are unchanged. '
. '
This amendment: becomes a p;1rt of and should be attached to the original
Permit.
HDL:go
\
Sine~2ly1
PJiginal Slflriilef (Fyf
t:EWIS R. MARTI~!
Lewis ll., l~tin
' . . " Central f i\e copy
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_£,,,; t!/fa,, '7
~tkm~ rfJ,chnundJmv gt, o//:{(1-u,wMV
. o/~ Yo//;;d,;,,,,,
fll ;1....., 6',.t-,.d,.,,v
&,/4 o/// o//f2Ln.wrvjf-.
March 11, .1975
Mr. Brock Nicholson
Chief Engineer
Air Quality Division
Department of Water & Air Resources
Raleigh, North Carolina 27611 ~--.,, Re: Permit No~
Dear Sir:
9. tJ. fg.,,,,, 2/17
//.9 J/4/4,,,,,k,.,, e/.t,..,£
a;,,,✓,JV -t. 2756'5
RECD MAR 1 2 1975.
According to information furnished me by IMI Warp Knits (NC)
Tue , Oxford, North Carolina, they are presently under a
dire.ctive to install emission control device on a tenter frame
by April JO, 1975. Since that directive has been issued, there
are extenuating circumstances which we would like to bring to
your attention.
Since August, 1974, they have had cutbacks amounting to as much
as 65% in production. I am sure you realize that they are
suffering therefrom in the economy a great deal.
Under the contract for natural gas services to IMI Warp Knits
(NC) Inc., Oxford, North Carolina, the Public Service Gas Company
of North Carolina is not required to guarantee an amount of gas
sufficient for the operation of the plant and in January and
February, 1975, they suffered a 35% curtailment in gas services.
The management feels that it is necessary that they install
certain standby equipment for propane gas and this is an additional
expens·e which they did not anticipate. The two expenses immedia-
tely would be more than they can financially withstand as a result
of the recent economic depressions.
In light of the before-mentioned situations which have arisen
since the previous directive was issued, IMI Warp Knits Inc.,
Oxford, North Carolina, respectfully requests that the deadline
Gopy
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~ (.91.9,) 6'.9.J-8/6/
k tJ/1-,,,/
o/1:diirui~ /],,;~= &t-o/flki1.1trr,/
o/~ Yo/~
~-i9'.-6-',a'-~
~ 'YI:" o//;{Jk,,.,v;;f-
Mr. Brock Nicholson -2-
9.tl.!JJ.-2111
11.9 Jt,-G',t,nakn/ e/,t,.,,/
4/~-ff -G'. ZJ56'5
March ll, l975
for the installation of emission control devices be extended
with the idea in mind that 'the present economic conditions
will improve to allow them to make this additional expenditure.
I do hope you will give this favorable consideration and in
the event there is any further correspondence in connection
herewith, I would appreciate you ·either contacting me or
Mr. Jim Patterson, Plant Engineer, IMI Warp Knits, Industry
Dr±ve, Oxford, North Carolina 27565.
Thanking you, I am,
WTW:phh
Cc: Mr. Jim Patterson
~e~
William T. Watkins
Attorney at Law
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NORTH CAROLINA DEPARTMENT OF WATER AND AIR RESOURCES
AIR QUALITY DIVISION
REQUEST FOR ACTION TO BE TAKEN
The item listed below. requires action to ascertain com1>liance under Article 21, Chapter 143 of the
General Statutes of North Carolina, concerning rules and regulations governing the control of air pollu-
tion:
Name
nu warp Knits
Subject
request for ext.ension of Permit 1/2097
Investigation Requested· By
NCF0
Remarks
Address .
Oxford
Address
original date o.f November 30, 1974 had been extended to April 30, 1975
Assigned To
ITlvestigated By Date
Melvin Flora 3/24/75
Action Recommended
schedule conference
Investigation Report
l. Contacted Mr. Jim Patterson, Plant Engineer.
County
Granville
County
Date
Returned
3/24/75
2. Mr. Patterson indicated that due to economic and energy reasons he wished to request
additional time to install his control equipment.
3. Mr. William Watkins, Attorney, was to send letter requesting additional time. (see
attached letter)
4. As the time required will.go pass the attainment date, a conference is suggested.
5. A letter was drafted (see attached) advising IMI of their position and our desire to
meet with them.
Correspondence To:
White-Engineering Branch; Yellow-Central File; Blue-Regional Office; Green-Engineering Branch
AQ-16 Rev. 7-1-71
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NORTH CAROLINA DEPARTMENT OF WATER AND AIR RESOURCES
AIR QUALITY DIVISION
REQUEST FOR ACTION TO BE TAKEN
The item listed below. requires action to ascertain compliance under Article
General Statutes of North Carolina, concerning rules and regulations governing
tion:
Old Name -IMI Warp Knits
Name ...... ~---.Criste;~, Inc.
_Address-···-···
Oxford
Subject_______ • _.
'l!.!lque~_for-additional year to achieve -;;~plian~~ ·· · -·
Investigation Requested By
North Central FO
Remarks
Address
21, Chapter 143 of the
the control of air pollu-
County
Gramrille
County
I V.E, violation of textile tentar frame
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Assigned To
North Cautral FO
IIlvestigated By
Melvin Flora
Action Recommended
Date
4-2/i-75
Enforcement action r·equired, L·e. Special Order by Consent
Investigation Report
Conference held· lri.th:
J:!.tl Potteracn, Plant En~ •• OY.ford c. J. O'Br7ont, E:7:~. V. P., Oxford s. J. Barricella, V, P., Mew York
Willi= Wal!c:'.ns, Attorney, Oxford
Date
Returned
4-29-'-75
Due to econ=ic an.1 cneri;y considerations, Criste::i: has found it desirable to request a one-
year ettension to achieve CJLtpliance.
Violation in qua!ltion is excessive v:'.sible emitJSiom:1 from a te::ttile tentering frame.
T!te policy of the fil'_G was e,q,J.nined in deta:1.1 and Cr1.stex officials were instntcted as to
procedures and requir=ents for entering into a Special Order by r.onscnt,
Cristex officials advi3ed t!lat within t:wo ,1ee!ts they would submit a request complete with
t:!l!le schedule, reasons, and docmnentation for an extension until October 31, 1976,
r Signature:
i ,nQ\·' t ... )' ?"'-·•"' i~, lJ
White-Engineering Branch; Yellow-Central File; BtulReg/onal Office; Green-Engineering Branch AQ-16 Rev. 7-1-71
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April 2, 1975
Mr,. Ji:a Patt.arson
Plnnt Engineer
-~Aari>~ '---ie1;h1et.1; l:>r1~e.
oxfc.rd, 1lc 27 565
Dezir Mr. Patterson:
SUBJECT: Request for =tension of Permit No. 2097
This letter is to acknowledge recei?t of correspondence received March 12,
1975 from Willi.am T. Watkins, Attorney nt Law, in the behalf of your position
aa it pertains to Air Quality Permit F.o. 2097. · Permit No. 2097 cun:eutly re-
quires controls to be installed on n tenter fr=e by A?ril JO, 1975. Mr. Watkins
indicated that due to certain economic aud energy considerations, the April JO,
1975 date is one that you can not financially withstand.
Suction 110 of the. ·Cle= M..r Act of l!:l70 providea that co.ch state devulop,
· adopt, and i.mpl1..'fileut a plnn "hich will assuru. compliance with the national air
quality st!l.Ildards within three (3} years of approv41 of the state's plan by the
Federal F.nvirocmentul Prot·ectio,1 Agency. Furthertnore, Section 110 provides that
c:;iission standards be :.,rescr:l.bed containi.-i.g time schedules· \,-nerehy each source is.
to conply with the~e et1ission. standards aa expeditiously as poasiblo. The l!orth
Carolina. Rufee and il.egulationsGoverning the Control of Air Pollution (paragraph
6.5} which is a part of the State's Ir.lplcmentation Plan was approved on Hay 31,
·197 2,· by the Federal· Environ::icntal Protection Agency; therefore, the· attail1lllent
data for compliance by all sources is May 31, 1975. The Federal Environmental
Frotection Agency-is under court ordur by the Federal. Courts not to.extend any
cor.i.pliance schedule beyond the attni=ent date; however, the Environmental Man-
agement Cocmdssion has adopted a policy for consideration of post-attainment data
compliance schedule involving use of special orders.
It appears that you will·be going beyond·May 31, 1975 in achioving .colll])liance.
According to Mr; \fatkins • s letter, the circwnstances requiring this extension·, are
econora.ica and the energy crisis. The facts that created those circumstances will,
of course, have to be documented by means of profit and loss statements, letters
fron the gas company, and/or othor doc=antation to support r-ur ;,oeition.
r<.r. Helvin Flora of this office has been
convenience during the month of April, 1975.
for post-attainment date schedules vith you.
shortly to arrange a conference.
instructed to r.ieet with you at your
He will discuss the policy adopted
:il:. Flora vill be contacting you
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Mr. Jim Patterson
Tbauk1ug you for ,uur cooperatio11, I am . .
CCI Mr, Brock Nicholsoa
Siucerel7,
~r
.. Marshall lackley
B.eaioual F.agineer
Air_Qualit7
April 2, !97S
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NORTH CAROLINA DEPARTMENT OF WATER AND AIR RESOURCES
AIR QUALITY DIVISION
REQUEST FOR ACTION TO BE TAKEN
The item listed below. requires action to ascertain compliance under Article 21, Chapter 143 of the
General Statutes of North Carolina, concerning rules and regulations governing the control of air pollu-
tion:
Name
IMI Warp Knits
Subject
Address
Oxford
Request foX' extena1nD of complet1oo date
Investigation Requested By Address
w. T, Watkins
Remarks
Conduct review and make recoJ:Imendations
Assigned To
Eng. Brancii/RRO
Il1veStigated By
Derr Leonhardt
Action Recommended
No Need to Revise Permit~ Send Letter
lnvestiga tion Report
Oxford
. Date
5/7/75
County
C11aaville
County
Granville
Date
12 Mar 75
Returned
5/7/75
1. IMI Warp Knits will be issued a Special Order to extend their construction
completion date.
2. There is no need to revise the Permit No. 2097R to reflect the extansion.
3. I recommend that a letter be sent to IMI Warp Knits explaining the situation.
Correspondence To:
White-Engineering Branch; Yellow-Central File; Blue-Regional Office; Green-Engineering Branch
AQ-16 Rev. 7-1-71
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Hr. William T. Watkins
Attoru,,y at L3v
Law Ofiices of Watkins,
Edmundson, and Wilkinson·
J;'. o. llo:;; 247.
119 HcCiblU(~ Street
Oxiord, North Carolina 27565
near Mr. liat!d.ns:
i • .....;
Reference is raade to your letter ofl1arch 11, 1975 to Brock M. Nicholson
requestina that the date for ittst.allaticn of equipoent covered un.ier Per.nit
No. :1.097R issued to DU 1-iarp Knits (NC) Inc., 0:..ford, North Carolina be
e.'t.tended.
lhl warp Knits :and our Raleigh r"'gional Office are currently nei;otiating
the tenia of such au extension. Upon.completion of these discussions, a Special
Order will be issued by The Environmental Managecant Corumission. The date
contained in this document will serve to extend the cohlpletion date required
in Permit tlo •. 2097:R. As stipulation (1) of Per.:ut t:o, 20971':. contains the
vhraae. 11or ·as thi:1. data raoy be r-..:::i;nc!ed" it will ::;ot be necessary to revi~e the
Permit itself. The Penl!t vil.l remain in effect providing that the terms of
the Speclal Order .are met.
If you ,,.....,-e any further questions regardin,:,; t::.is matter, feel free to
contact Mr. Derr Leon.\ardt of this Office a.t (919) 829-1,740, e.-<tension 242.
Your cooperation is appreciatoo.
iiDL/b:;p
cc: l1r. Jii:1 Patterson, l'lant Engineer
L'il Warp Knita
Industry Drive
Oluord, NC 27565
Sincerely, ~
~ .
John D, Romans
Plans Review Coordinator
Air Quality Section
' Centra\
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TO: Marshall Rackley
Regional Engineer
Division of Envirownental Management
North Central Fie1d Office
Air Quality Section
Telephone: [phone]
June 16, 1975
FROM: Melvin Flora · ~ 1---
Engineering Technician ·-•-·· ... ,--------·-···· ...---... . --· . ·, -.... ··---... _ •--
SUBJECT: (_cristex, Inc. (Formerly IMI Warp Knits) ··'·---, Oxford·; North Cari>Tioa ____ :,..___ --·-· ... ·"
Special Order by· Cooaent
Attached you will find an AQ-16 with my recommendation for issuance of
a Special Order by Consent. · · ·
Io order that you be aware of our past history with Crietex the following
. is a brief description of events leading to the present ~ituationz
1. February 1973-
August 1973
2. August 30, 1973
3. February 15, 1974
. 5, April 24, 1974
Registration conducted,
Temporary Permit Application issued and
received for Visible Emission on tenter
frame, Final date -June 30, 1974 •.
Request for revision of T~rary Permit
Application.to reflect fillal date of·
November 30, 1974, _This detenwi.ed after
Hill Enviromnental Group conducted tests·
·snd submitted proposal,
Temporary l'ermit No. 2428 1.a~~ with fiMl. ·.
date _of Juiie 1, 1974. ·. · .. · · · ·
Received AQ-22 for SpieJIIIIBII mist eliminator ·
snd. heat recovery system.
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. . 1\11 ···. Memo .to Marshall Rackley ..
... ,June_ 13, _1975
Page 2
6. May 9, 1974
7, . Novenber 24, 1975
8. December 10, 1974
December 17, 1974
February 17, 1975
9. February 17, 1975
10; March 12, 1975
11. April 2,· 1975
12, April 24, 1975
13. May 7, 1975
14. · May 27, 1975
SUMMARY:
.. -. · .. ··-
Issued Permit No. 2097 for proposed equipment.
with installation date, November 30, -1974,
(This effectively revised Temporary Permit.
No. 2428).
Request revision of Permit No. 2097 to allow
for._energy redu<.:tion study (their natural gas
was being curtailed) until April 30, 1975.
Regional AQ--16 concurring with revision
Plans Review AQ-16 concurring
Issued revision · ·
Il!I advised of serious economic aud energy
problems that would require additional time_
for compliMce.
Received fon;,al notice of desire to extend
compliance schedule (submitted by Attorney
Watkins)·.
Our letter advising of post-attainment policy
and desire· to.hold conference.
Conference with lMI executives and atforney.
Discussed docW!lentation and time schedule.
Plans review sent Criste: letter advising that
. a Special Order by Consent would amend their
Permit and Permit would.remain in.effect.
• Received formal r~que~t for extension until
. October 30, 1976 with supporting documentation.
At this time Cristex has shown good faith (Permit application and tests) in
their intentions of cQmply:!.ns with Regulation No. 2, .. The company has proceeded.
according to oui directions duri.ns a trying i::lme for their industry~ I feel
that their request for time is legitimate·and·therefore recommtmd the ·issuance
of the attached_ Special, Order, ·
.I also recOlllClend that the Perinit be t~sed to reflect a December 31, 1979
expiration.date instead of_ December 31, 1977.
MF1jc
·Attachment Central Fi1e Cop~
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CERTIFIED MAIL
.RETURN RECEIPT REQUESTED
:Mr. C. J. O'Bryant
Vice resident
. Cristex, nc.
· Industry Drive
Oxford, North Carlina 27565
August 12, 1975
Subject: Special Order
AQ-75 -055
You are .hereby advised ·that your tenter frame number one is being operated in
violation· of Regulation No. 2, "Control and Prohibition of Visible Emissions" and
is operating without the expressed or implied permission of the Environmental
Management Commission.
The final date by which North Carolina sources were to be·in compliance with
applicable emission standards was May 31, 1975. Recognizing that not all North.
Carolina sources would be in compliance by May 31, 1975, the Environmental Management
Commission adopted a policy which would allow certain sources to continue· discharging
air contaminants in violation of emission standards pursuant to an enforcement order
or other enforcement. procedures deemed appropriate by this Division.
Enclosed you will find a Special Order by Consent which, when execuced by
Cristex, Inc. and approved by the Environmental Management Commission, would allow
for tte orderly compliance with Regulation No. 2 by October 30, 1976, which in our
view is a reasonable amount of time. Please e.~ecute the Special Order by Consent,
· and return the original and one copy within twenty (20) days. of receipt. Should you
not agree with the terms and conditions of the Order, please discuss any objections
with our Regional Engineer, Mr. Marshall Rackley, telephone number [phone].
If after discussing the Order with Mr •. Rackley, you are still unable to. agree with
. the terms and conditions of the Order, please note that you will have the opportunity
to appear .at an adjudicatory hearing to show cause why the Order,. in whole or in part,·
should not be issued.
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· Mr. C. J •· O' Bryant
Page 2
August. 12, 1975
·Also, notice of intent to.issue the attached Special Order by Consent,
requesting public comment on the proposed order, will be published in the Raleigh
News and Observer in accordance with the Environmental Management Commission's
Policy and Federal Regulations.
DMR.:jc
. : . Enclosure
.cc: Mr. M. W. Puette
.. Mr •. J. · A. McColman
Mr. Brock.Nicholson
Mr.· Marshall Rackley
Lewis R •. Martin
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NORTH CAROLINA
GRANVILLE COUNTY
IN THE MATTER OF UNAUTHORIZED
DISCHARGES OF AIR POLLUTANTS
TO THE AMBIENT ATMOSPHERE BY
CRISTE.X, INC. , OXFORD, GRANVILLE
COUNTY, NORTH CAROLINA
SPECIAL ORDER BY CONSENT
AQ-75 -055
. THIS ORDER ·BY CO.NSENT made and ei:itere<l into pursuant to North Carolina General
Statute 143-215.110 by Criste.'<, Inc., hereinafter refe=ed to as the COMPANY, with
the North Carolina Environmental Management Commission,· an agency of .the State of
North Carolina, hereinafter known as the COMMISSION.
• WITNESSETH:
I. The COMPANY does •hereby stipulate as follows: ..
A. The COMPANY has operated and is now operating tenter frame number one at
its facility at Oxford, North.Carolina.
B. The COMPANY has.continuously discharged and is now discharging visible
emissions from tenter frame number one in violation of Regulation No. 2,
"Control and Prohibition of Visible Emissions".
C. The COMMISSION issued Permit No. 2097 to the COMPANY on May 9, 1974 for the
construction and operation of a mist el:illlinator installed on the exhaust of
.tenter frame number one.
II. The COMPANY desiring to comply with the legal requiremen.ts of the COMMISSION
regacding visible emissions to the ambient atmosphere and with all pertinent
provisions of the law and applicable rules and regulations of the COMMISSION
does hereby agree to do and perform all of the following things on or before
the dates hereinafter set out:
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. SPECIAL ORDER BY CONSE.i.'IT
Page 2
A.
. B.
C.
·III.. The
Enter into a purchase contract or other agreement for the installation of
air pollution abatement equipment on or before June 1, 1976i
Begin constr_uction of air pollution abatement equipment on or before
September 30, 1976.
Achieve compliance with Regulation No. 2, "Control and .~::h,~itiof"i~'() ',i
Visible Emissions", in the manner chosen and proposed b';'.,.t~t. ~.W J '(
. -\ .. ':' • 'l'.· . -,, ~ \ •·& . .
Pe.rmit No •. 2097 on or ·before October~, -1m·t ; · "\ V. . . .
COMPANY ~hal{ operate and maintain i . ~\}
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~~:w;:•s: as to min:iJD.ize the
. : -. . . . . . ' . . . .
. .
impact of visible emissions during the period between the date this Order is
_executed by the COMPANY and the date specified in this.Order for achieving
· compliance with Regulation No. 2, "Control and Prohibi.tion of Visible Emissions".
In rio case shall the rate of emissions be increased over-those resulting from
full production or firing rate existing on the date this Order is executed by
the COMPANY ..
_IV. The COMPANY agrees .that this Special Order shall pertain only to that equipment
· o; source described in Section I.A. of this Order. Unless an applicable
Special Order or Permit has been issued by the COMMISSION, any violations of
Air Quality Standards, resulting from other sources or equipment for which
the COMPANY is responsible shall subject the COMPANY _to all. sanctions provided
_by North. Carolina General Statute 143-215 .114.
·v. Failure of the COMPANY to comply with any provisions contained herein, including
Section III, or discharges from the tenter frame number one after October 30,
1976 in excess of applicable standards shall subject_ the COMPANY to all sanctions
provided by North Carolina.General Statute 143-215.114.
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SPECIAL ORDER BY CONS&"'IT
Page 3
This the ______ day of ___________ , 1975. ·
· ATTESTED:
, APPROVED AND ACCEPTED
BY: ____________ _
P. Greer Johnson, Chairman
Water & Air ·Quality Control
Date: ------------
CRISTEX, INC.
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NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT
AIR QUALITY-SECTION -··---
REQUEST FOR ACTION TO BE TAKEN
The item listed below. requires action to ascertain compliance under Article 21, Chapter 143 of the
I General Statutes of North Carolina, concerning rules and regulations governing the control of air pollu-
tion:
~ Name C;~stex
"-.5.l!..bjest;· ·-;--· .... _ ,; , ..
·---~ Address
Oxford
County
Granville
I __ .,_R'-'e"'q,_,u00e,..,s'-'t"--'· f"o"'r'--"'e"'xt=e"'n""s"'i"'o"'n,___,o'-'f'-'S'-'O'-'C"--'d"'a"'t=e-"s _________________________ _
Investigation Requested By
I !!CFO
Remarks
I Assigned To
NCFO
I Illvestigated By .
Melvin Flora
Action· Recommended
I Prepare facts to submit to commission
Investigation Report
Address County
Date
Date Returned
4-30-76 5-4-76
I 1. Contacted Mr. C. J. 0' Bryant, Plant Manager and· Mr. Jim Patterson, Plant Engineer.
2. Conducted a tour of plant to determine necessity for beamed yarn.
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3. Contacted Celanese and American Enka to confirm unavailability of beamed nylon yar ..
4. Requested Cristex to submit breakdown of cost for beaming operation.
5. Cristex officials concerned as to whether we would fine them if they failed to meet
dates-without formal approval of extension request.
6. Prepared memo of status to advise Marshall Rackley, Regional Engineer, of current
status of Cristex.
I White-Engineering Branch;
~Q-16 Rev. 7-1-71
Yellow-Central File; Blue-Regional Office
1-----
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Cristex Corporation, Industry Drive, Oxford, N. Carolina 27565, [phone]
May 4, 1976
Mr. Melvin Flora
Air Oualitv Division
Department of Water & Air Resources
Raleigh, North Carolina 27611
sueJECT: NORTH CAROLINA ENVIRONMENTAL MANAGEMENT
COMMISSION, PERMIT NO. 2n97
REFERENCE: OUK LETTER OF MARCH 29, 1976.
Dear Mr. Flora:
Pursuant to our meeting on Friday, April 30, 1976,
a summary of the costs Cristex Corporation is incurring
in establishing a fiber warping operation is listed
below.
In order to satisfy our requirements for beamed
yarn, it is necessary to install four (4) warping units.
A warper unit consists primarily of a warper, a creel
equipped with electronic tensioning devices, an electronic
scanner for quality control purposes, and auxiliary
equipment such as eveboards and static electricity eliminator
bars. Costs of these units vary depending on installation
of rehabilitated used equipment or purchased new equipment.
Equipment
#1 Warping Unit
112 Warping Unit
#3 Warping Unit
#4 Warping Unit
500 Aluminum Beams
500 Steel Beam Racks
Beam maintenance and
repair unit
Installed Cost
$ 40,939,00
45,185.00
69,015.00
99,215.00
178,500.00
46,375.00
7,500.00
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Inst~llation costs
(Mechanical~ Electrical)
Equipment Total
7,756.00
$ 494,485.00
Purchased a 3n,408 sq. ft. used
manufacturing plant complete with
required air conditioning equipment,
located in Butner, N. C. 607,000.00
GRAND TOTAL $1,101,485.00
We have requested Celanese Corporation to furnish
us a statement ~erifying the fact they will discontinue
the manufacture of textile denier nylon on or around
July 1, 1976.
As mentioned in our meeting, we deeply appreciate
the cooperation and attention given to our request and
hope to receive favorable consideration.
CJO/mgo
Yours truly,
Q-,,,-7. ,,-,,1L-? · t-, -v --x· -#,, y;:: l ·. _,,t</c-zv1.-,
-/.' /7 c./ J. O'Brvarff: -V Executive Vice President
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Division of Environmental Management
North Central Field Office
Air Quaiity.Section
Telephone: [phone]
May 10, 1976
MEMORANDUM
TO: Marshall Rackley
FROM: · Melvin Flora -),· /
SUBJECT: Cristex Corporation; Request for extension of time of SOC AQ-
75-055
Attached you will find a extension request from Cristex dated March
29, 1976, To confirm Mr; O'Bryantll position Ron Hawks contacted Celanese
Corporation. Celanese supported Mr. O'Bryanth statements. Ron also called
American Enka, a supplier of nylon yarn, and they too confirmed the problem.
in b~d yarn. ·
;
Cristex was visited by Ron Hawks and myself to discuss the matter fur~
ther on April 30,· 1976. The cost or beaming their own nylon yarn was ex-
plained and coni'irmed by their letter of May 4, 1976,
It is apparent that Cristex has a real problem.that will require substan-
tial. investment to solve •. They have asked for 18 months delay. The particular
reasoning ·for 18 months hasn't been.discussed as I feel this would indicate.
• regional approval of ext.ension request. Before additional dates for compliance
can be negiotiated·someone needs to indicate approval of request.
. As history for .this request Cristex has been given a previous· extension
· ot 18 months· .·due to the energy crisis and a need to convert fuel types. Thia
is a area source. The violation is VE. from a tenter. frame. ·
MF:dap
Attachment
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D
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. Division .. of Enviroronental Management
:-iorth £entral Field Office
MEMORANDUM
TO: John Romana
Air Quality Section
Telephone: [phone]
M.ay 13, 1976
FROM: Marshall Rack.lay 'Jtl /(
SUBJECT: Criatex Corporation; rcquent for extension of SOC AQ-75-O55
Ple:13e refer to tho following documents that are ,'llr ... ady Ml file:
(1) E-16-, 75 memo of '!elvin Flora . (2) !!pacial Order Aq-75-O55 ('.3)
Grbtmx lotter of 3-29-76 (4) Criatex letter of 5-4-76, (5) 5-10--76
!ll<!mo of ,fol•1in Flora,
You will nott: that Gristex had originally plBnned to nchievn cor.i-·
pliance with vi1111,lc &lllission by }'.ovric,ber 3(), 1974, Jlowever,. energy and
econom1.c con,iitleratione caused tli<!. co:o;:,:my to r!!q11est a delay until October
3il, 1'176 '<hich hocame the compl1:1cce dato, in SOC Al.)-75-055, In thoi-i: lotter
of 3-29-76 tho compan:1 hns requested ;in 18 month delo.y in that the company
bllG co· invest a lllillion dollars to continue operation.
An indico.ted in Hulvin' a rJe::,o of 5-10-76. ,:e h,we deteniined that the
situation as presented by corapany conccrninq tho neod for buying new e~uip-
ment and l!11c1litie,1 is accurate. ·Tt,erefore, th1:1 qut1stion that° remains ii:
tho matter o~ is it reasonable to allow the company to delay installation.
of the control e,wipr.ient (which costs approxilll8toly $70,000 arid the com-.
pany haa been aw:11:e of this ·expenditure for ·at loaot 2 yoar11) as o t'eault .
of a need to speft.l $1,il:OO,OOO in the iffllllediate futi)re. Io that we CM not
truly evaluate _the izapact of the new expanses on the company, it ~kes. it
necessary for us to rocOl!l!llond that tllic requost be carried to the Commission
for a determination,
.In my judi;t'l!llant it is poasibl11 that the COJ!ll)eny would follow through
vith inetAlling thtt equipme11t vith &Ollle ·short delay if their request· WIiia
denied. llowever, I have nothing fir•, .to base such a judgement oii. Alao
: the amount of tb,e request ad Juis not been tied to any apocifie c,vent aruf aa
a alternative to taking the request to _the C0m111isaion at thia point, it may
be possible to nagotiato the time.
Kll1dap
cc: Bl'ock :acholaon
Craig Bl'0111by '.'.. . . '
Central file Copy ~ ~ ~[;'~1
.~·,.,,.. . .'
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TO,
THROUGH:
DIVISION OF l':NVIRoma,NTl'L !IA.'11'.GE:ME?IT
IUR QUALITY SECTION
. May 26, 197&
Mr. James A, Mccalman, Chief
Air Quality. Section.~
Brock Nicholllo~
F!<OM, John Romans 91{
·suBJECT, Cristex.corporetion, Oxford
Extension Request for Special Ordor AQ-75-055
Crixtex has requested an 18-t:>Onth extension of the final compliance date for
installation of visible 81>\ission controls.
Crixtex wae issued a Tmaporary Permit to expire on June 1, 1974. Thi& Temporary
Permit was effectively extended by subsequent issuance of a Permit until Novo&lber
30, 1974. This Permit was then extended to.April·Jo; 1975. Spe~ial Order AQ-75-
055 was later issued allowing until October 30, 1976 for .. installation of controls.
'rho. reason expressed by Crixtex .for the present extension request is the
neces11ity· to expend a great doel of capital·on production equipment replacements.
'These replacements are due to. a recent change· in the for111 of the yarn supplied to
crixtex. 'l'hi~ change has biten confimed to be .t,eyond the control cit Crixtox.
Tho capital necessary· to effoct this production equipment change is 1.1.
million dollars. The eatirnated cost .of the controi equipment is 70 thousand
dollars, an expenditure that crixtax has );,eon. aware of-for· sevaral years.
I presume.then that crixtex.is basing their extension request on:capital
flov problem&, a situation vhich Marshall Rackley and I feel i!' J;eyond, the 'staff' 11 .
llbility to accurately evaluate:··_ ·Extensions should only be ·granted due to •.-'
extenuati~g_ circ11111stanoes beyond the' control of tho source.: .,
. : •·; .... ,
. :/•rho-flo;,,•,of capital i's not beyond the ·control of the coinpeny,
since,· the . control costs liave, been known for vell over a year; :
., .. '·,·.\ ,' .;,;_,_ . ,. \ ,. ~" ., . ·-
_ particulary ·,
. . . ' -
1·, therefore, request that Crixtex be. noUfie&d that this Divisio·n does· ne>t ' _,·
agree with:-the request 'and intonda to enforce the existing s.,;.cial order cOlllpliance •
date'of Octo~er 30, 1976 •. . , ,
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Cristex Corporation, Industry Drive, Oxford, N. Carolina 27565, [phone]
July 19, 1976
Mr. W. E. Knight, Director
Department of N. C. Natural & Economic Resources
Box 27687
Raleigh, North Carolina 27611
SUBJECT:· NORTH CAROLINA ENVIROIIMENTAL MANAGEMENT
COMMISSION, PERMIT NO. 2097.
Dear Mr. Knight:
We are in receipt of your letter denying our request
for an eighteen (18) month extension to subject Permit No.
2097. We are disappointed that we did not receive favorabie
consideration of our request as our company is being subjected
to serious capital proble!!'S as described in our letter of
application. None the less, we will strive to 6omply as
directed by your department.
As per your instructions, the writer met with your
Mr. Marshall Rackley on Friday, July 16, 1976 to discuss
our schedule for installing ~quipment. ~e agreed upon a
time schedule (copy included) as submitted to us by our
contractor, Piedmont Energy System, Inc. Mr. Rackley agreed
tc ~ safety factor date of around January 15, 1977 in view
of the fact that the December 17, 1976 date was in the
hciliday season. However, we will strive to meet the
.December 17,.1976 _da.te if a.tall possible.
CJO/mgo
Enclosure
cc: Mr. Marshall Rackley
AIR QUALITY DIVISION
CENTRAL OFFICE
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July 30_
August 13
August 20
October 15
. October 29
November 1
?/J\(<'.,._.J,iv /.)
November 26
December 17
CRISTEX CORPORATION
I~STALLATION SCHEDULE
Received Purchase Order and Deposit
Receive Drawing Approval
P. O.' BOX 3933
GASTONIA. N. C. 28052
[phone]
Complete Purchase Orders For· Components
Receive Domponents
Complete Assembly0,of Components
Ship System /,eJfl! {v,i;-f ,,..._,f/ ... l
Complete Installation
Complete System Start-~p and De~bugging.
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MEMORANDUM
TO: John Romans
Division of Envir(i;;:~ental Manageaent·
-North--central Field Office
Air Quality Section
Telephone [phone]-
July 22, 1976
FROM: Harohall Rackley ,W.lf
. -<~/~/,/ __ i;,~-·;-,:~---~-:::~':
. ) I
1· SUBJECT:. Special Order of Consent, AQ 75-055, Cristex, Inc,, Oxford
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·In. reference<' to the ottached copy of a letter to Mr, Knight from Cristex,
I am recommending ·that the above referenced Special Order of Consent be modif_ied
aa follows: ·
~ill: ch
Part II A -Contract let by July_ 30,·1976
B -Construction begun_ by :fovember 15, 197_6
C -Achieve compliance by January 15, 1976
If there are any questions, contact Helvin or myself.
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NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT
AIR QUALITY SECTION
' • > --.--•••••' < •'• .,,T ' • •y ' • •• • • ' •
REQUEST FOR ACTION TO BE TAKEN
The item listed below requires action to ascertain compliance under Article 21, Chapter _143 of the--
General Statutes of North Carolina, concerning rules and regulations governinv, the control of air pollu-
tion:
Il1vestigation Hequested By
North Central Field Office_
~-c Oxford _)
Addre~s
Counly
Granville
County
------------------------------------Rem arks
Assigned To
North Central Field office
ITlvestigated By
Melvin Flora
Action Recommended.
Inspect for compliance 11/15/77.
Investigation Report
Dau,
ii/29/76
1. Received call from Jim Patterson, plant engineer.
Date
Returned
11/29/76
2.
3.
4.
Mist eliminator unit set on roof, heat exchanger to be set this week.
Expects to meet final compliance prior to 1/15/77.
Original SOC allowed until 10/31/76. They requested 18 months extenston and
we advised to install As soon as possible.
Central :.'-1;. t;
Correspondence To: --------------------------------------------------
Signature:
White-Engineering Branch; Yello~-Central File; Blue-Regional Office
AQ-16 Rev. 7-1~71
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NORTH CAROLINA
BOARD OF WATER AND AIR RESOURCES
·· RALEIGH
APPLICATION FOR APPROVAL OF
PLANS AND ISSUANCE OF
A "PERMIT"
TO CONSTRUCT AND OPERATE AIR
POLLUTION ABATEMENT FACILITIES AND/OR EMISSION SOURCES
Filed By: _.i..Ccc.91JJc..Sc,_,'.1.I'.cEX""----'c"'o_,.5..u.P~-~---
(Name)
INDUSTRY DRIVE
(Address)
OXFORD, N C
AQ-22 Rev. B/72
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NORTH CAROLI NA
BOARO OF WATER AND AIR RESOURCES
Raleigh
APPLICATION FOR A "PERMIT"
To Construct and Operate Air Pollution Abatement Facilities and/or Emission Sources
Three Copies to be Submitted
Fourth Copy Should be Retained by Applicant
To: Board· of Water and Air Resources
P. 0. Box 27687
Raleigh. North Carolina 27611 Date: -~l"--=-...5c:-CJ7~7'------
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, application
in the County of Granvil J e at t · Drive Oxford N.C. •c-om_p_a_n_y_i~f-A"p-p"l-ic-a'b"l~e) Street and Ci y or Town Address of Plant or acility
for issuance of a "Pennit" to construct and operate air pollution abatement facilities and/or emissions sources at above
location as specified in the accompanying drawings, specifications, and other pertinent data:
1. Nature of Operation Conducted at the Above Facility: Textile Knitting, Dyeing, & Finishing
2. Description of Process{es) Whose Emission{s) is/are to be Controlled by the Facility or Source{s) Which is/are to be
Constructed or AHered. (Complete Section I) Beam Dyein·:,;-6 Atmospheric Tubs
3. Furnish Type and Na rra ti ve Description of Proposed Contra 1 Device { s). { Comp 1 ete Appropriate Supp 1 ementa 1 Data Sheets for
Control Device to be Installed and/or Operated. Include Make and Model Number of Control Device{s) and Number of
Identical Units). None -
4. Contaminant
Emitted:
Weight Rate of Emissions {lb/hr):
Without Control Device With Control Device
Hydro-Carbons
5. Name and Address of Engineering Firm that Prepared Plans:
Gas ton County (Dye Tub Manuf actor)
Control Efficiency (%):
Without Control Device With Control Device
6. Ultimate Disposition of Collected Pollutants: 7. Date on Which Facilities are to be Completed and in Operation:
8. Indicate Period of Time for Which Facilities
are Estimated to be Adequate: __ Years
Name:
{Responsible Individual of Company Purchasing/
Operating Facility ... PLEASE PRINT)
AQ-22 Rev. 8/72
__ __.,_.,,_ _____ , 19 __ _
9. Estimate Cost of Air Pollution Control Device $ _____ _
Mailing Addr~ss: Cristex Corp.
Industry Drive
Oxfo,.,d, N.C. 27565
Telephone Number: 919-69 3-611+1
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I. GENERAL DATA FOR PROCESSES
• Atta.ch de.ta.i..led pJt.Oc.Uh e.ng.i.ne.Vling CVLawbtgh, e.quiµne.n.t dlta.wirtgh a.nd 6£.ow dia.glt.amh Qo1t. the. pl!.OC.e.hh ( u 1 O/t. tiouJtc.e. (6 l
bei..ng c.on..6tlw.Ued 0/t. a.Ue1te.d.
Name of Process: 6 Atmosoheric Dye Tubs
Total Weight of Materials Entering this Process: J Baa lb/hr or ton/hr Nylon/Acetate Cloth
Volume and Temperature of Air Flow Entering Control De\1ice: _____ CFM@ ____ 'F
Volume and Temperature of Effluent at Discharge Point to Atmosphere: CFM@ ____ 'F
Po 11 utant ( s) tc be Contra 11 ed: --'H,._·-'-,d"-"r_,o...:::.-_,Cc,ae.r,._,bc,o"-'-'n"'s'---------~---------
Ab G d L l ft Inside area of Stack _____ ft2. Height of Process Stack or Vent ave roun eve _____ .
Particulate Emission Rate {Before Control) lb/hr
Particle Size Distribution: O-5p __ ~• 5-lOp__l!, 1O-2Oµ__..l!, 2O-3Oµ__..l!, 3O-4Op__l!,_4O-5Op__l!,>5Oµ_____z
Gaseous Emission(s): Name {Chemical Formula)
See·Attached:
or 1 b/hr
II. SUPPLEMENTARY DATA FOR INCINERATORS
Circle Type of Waste or Indicate Composition: Type 0 Type I Type II Type III Type IV
Combustible: ___ % Non-Combustible: ___ % Moisture: % Heat Value: __ BTU/lb
Total Waste Gerierated Per Day: lb. Hours Incinerator will be Operated: ____ hrs/day
Design Capacity for Above Waste: ____ lbs/hr Manufacturer and Model Number; Approximate Cost:
Primary Chamber Volume: ft.3 Secondary Chamber Volume: ft. 3
Air Requirements: Total Excess Air __ % Draft: Natural Induced Other
Overfire Air: cfm Underfire Air: cfm
Flame Port Temperature: °F Secondary Chamber Temperature: °F
Stack: Inside Area __ ft.2 Height __ ft. Gas Velocity __ ft/sec Temperature °F Fan Capacity __ cfm Stack Lined? ___ _
Is there a Wet Scrubber?
Yes No Flow Rate of H2O into Scrubber _gal/min . Temperature Before Scrubber 'F
Aux. Fuel: Oil Gas Other Burner Rating: Primary Chamber
____ .BTU/hr
Preheating Time:
Secondary Chamber
----~BTU/hr
---~m.in.
Stack
__ BTU/hr
Primary Burner: ls there a Preheat Timer? Yes No
Secondary Burner or Afterburner: Is there a Timer? Yes No Length of Time Burner is Operated ___ min.
Is the Timer Reset by Charging Door? Yes No Other Mode of Burner Control
Type of Feed: Manual Automatic If Automatic, Describe ____________________ _
Signature: Title:
.? f.'"'~ a ·~
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III. SUPPLEMENTARY DATA FOR FUEL BURNING SOURCES
• Atta.cit de..t.a,;1.e.d. d.{J)le.M.i.one.d d,uwfog 01t 6k.e.-tclt 6/iowing inteJtnal 6ea.tu.,'teli 06 dJtlje,'W,, wood OIL c.oa.1. 6i.lte.d boile.lL6. a.nd
,te.c.ovuy bo i.te:u,.
I Type of ~uel Burning Source _________ _ Stack Height Above Ground level ft. Inside Area of Stack ft2
Make and Model Number ____________ _ Volume of Furnace ft3
I Specify Actual .Amount of Each Fuel Used in Above Source (s):
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Oil Grade __ Amount __ gal/hr, at __ BTU/gal and __ lb/gal or lb/hr Coal __ lb/hr;
Wood lb/hr; Natural Gas SCF /hr, at BTU/SCF; Other ___________________ _
(Specify type. amount and heating value)
~
Specify Maximum Rating for Each Fuel Burning Source:
Coa 1 Oil Wood Natura 1 Gas Other __________________ _
Maximum Sulfur Content of Fuel %
Type of Sol id Fuel Burning Equipment Used: Hand Fired
Stoker Fired with Ash Reinjection Traveling Grate
Spreader Stoker
Pulverizer
Underfeed Stoker
Cyclone Furnace
Chain Grate
Other (Specify) ______ _
Ash Content of Fuel: Specify Method and Schedule of Tube Cleaning. if Applicable:
Coal % Wood % Other % Lancing Tube Blowing _______ Schedule ______ _
Emission Control Equipment (Describe in Detail in Sections IV and V)
Collection Device: Wet Dry Steam Injection Air Injection
Total Number of Fuel Burning Sources Within Property Boundaries:
Maximum Capacity Rating, by Type, for All Fuel Burning Units Excluding that Itemized Above: (Total Like Units)
Coal lb/hr Wood 1 b/hr Qi l gal/hr Natural Gas SCF /hr
IV. SUPPLEMENTARY DATA FOR WET COLLECTION DEVICES
*A.tta.ch de..ta..iJ'.ed e.ng,inee.,t.-i.ng d.'UW.lingf.> 06 the. co1itJt0£. de.vice. a.nd pa,'I..Uc.le. J,lze. vvwu.& Jtemova.1 e66,i.c.ie.ncy cwr.ve..6.
Liquid Scrubbing Medium and Additives:
Total Liquid Injection.Rate (Include Recirculated and Make-up Rates} gal/min or gal/1000 ftl
Operating Pressure Drop Across Device __ in HzO
ANSWER FOLLOWING QUESTIONS FOR SPECIFIC DEVICE:
VENTURI SCURBBER: Inlet Area in2 Throat Area in2 Throat Velocity ft/sec
GRAVITY SPRAY CHAMBER: Number of Nozzles Liquid Droplet Size u Co-Current Countercurrent
WET CYCLONE: PACKED TOWER OR PLATE TOWER:
Body Diameter in Length ____ in Cross-Sectional Area _____ ft2 Type of Plate ______ _
Inlet Area in2 Number of Nozzles ----length ___________ ft Depth of Packing _____ _
Outlet Area in2 Number of Plates_______ Type of Packing _____ _
OTHER WET COLLECTION DEVICES: GIVE COMPLETE DESC~ON!N-C(~Dik.:oE?IGN J'ARA~ITTR's ~ND DETAil'tl) ENGINEERING DRAWINGS.
. "· _j ~ .. _,.. . .. : .. / <·-~ 1 t·,. f .J /~1 t . -t"\. ri l l
·~.J \
Signature: Title:
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V. SUPPLEMENTARY DATA FDR DRY COLLECTION DEVICES
*A.:ttil.c.h de,,ta.,if_e.d engi.neVU.ng dltawi.;ig~ 06 .the co;Wtol device a.nd. pa,'t.U.c.£e. .6-i.ze v~M 11.emova.l. e6Qi.Ue11cy c.Wtvu.
Bag Material BAGHDUSES: Cloth Area ----n2
Number of Compartments Pressure -Drop Total ________ in H20
Method of Cleaning ________ _ Air-to-Cloth Ratio _________ ft/min
Time Between Cleaning mins, hrs
ELECTROSTATIC PREC!PITATDRS:
GENERAL:
ft2 Effective Area of Grounded Collector Plates
NL:,::ber of Compartments or Chambers Number of Cells per Compartment _____ _
Electrical Field Gradient at the Discharge or Emitting Electrodes _____ KV/in
Average Electrical Field Gradient at the the Grounded Collecting Electrodes ____ KV/in
Fields of Treatment ____ Potential Applied to Emitting Wires ____ KV
SINGLE STAGE TYPE:
Distance Between Emitting Wires and Collecting Plates _____ in.
Number of Isolatable Bus Sections _____ Corona Power ____ Watts/1000 cfm
TWO STAGE TYPE:
Distance Between First Stage Emitting Electrodes and Field Receiver Electrodes (Ground) ____ in
Potential Applied to Second Stage Emitting Plates ____ KV
Distance Between Second Stage Emitting Plates and Grounded Collection Plates ____ in
CYCLDNES/MULTICYCLDNES:
Simple Cyclone Multi cyclone Diameter _________ _ in Diameter in
Inlet Dimensions ______ _ Inlet Dimensions of Individual Cyclone
Outlet Dimensions ______ _ Outlet Dimensions of Individual Cyclone
Pressure Drop ______ _ in HzO Pressure Drop in H20
Number of Cyclones. ______ _ Number of Cyclones
OTHER DRY COLLECTION DEVICES: GIVE COMPLETE DETAILED ENGINEERING DESCRIPTION AND ORAWINGS.
Signature: Title:
-

4

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VI. AREA DIAGRAM
- ------·
O.,ner __ LC.c1?1.ILS::,.:.:'":.iFX,.z._-1.C;,.Q1-T"l=P!..Ot.:S:1.A!l..J.T:JI.!.01-Nil!• ____ _
• Location INDUS'l''l' VS, OXFQ3D, N.C. Give Street A .,
INSTRUCTIONS:
1. Show all surrounding buildings and roads within
1000 feet of subject equipment which is located
at center of circles.
2. Indicate location and type of building by the
use of small numbered circles with the de-
scription below.
3. Show roads as lines representing the road edges.
Indicate street names and highway numbers.
4. Show wooded or cleared areas by approximate
bounr'·ry lines and the words "woods 11 , "cleared11 ,
"cornfi e 1 d" 1 etc.
5. Indicate direction of north by arrow.·
CODE
G)
®
@
©
®
®
(J)
®
®
®
EXAMPLE
DESCRIPTION
-Cristex Corporation
Office
Boiler Room
G). Church
® Residence
X Indicates location of equip!llent.
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1.
2.
3.
4: s.
6.
7.
3;
9.
10.
11.
12.
13.
15.
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
27.
2r.: v.
DYE CHEMICAL
Nylofixan p
Sandacid V
Lyo'sen BE
Sando gen NH
Lyogen HN
Cenegen CJ
C.;Ques t
Dispersant A
C-Clean RA
C-Lube MW
Neutral #9
Pomoco Q-48
Cindet 542
Chemfume
Cottacid
MANUFACTOR
Sandoz
II
II
II
II
Crompton & Knowles
Chris Tex Chemicals
II
II
II
W. F. J<7 ancourt
Piedmont Chemical Co.
Cindet Chemicals, Inc.
C!-iemonic Ind.
Prescott Inc./ Chemicals
Mono Sodium Pyrophosphate
Worth Chemical Co.
Acetic Acid ( 56%) II
Aqua Amr:ionia II
Formic Acid II
Muriatic Acid II
Soda Ash II
Soduim Hydrosulfite II
Caustic Soda II
Tannie Acid II
Tartar Emetic II
Sodium Nitrite II
Sodium Hypochlorite II
Nitric Acid II
, ........ ., ;
4000 Monroe
Charlotte,
II
II
If:
II
Road
N.C. 28205
P.O. Box i988
Charlotte, N.C. 28201
P.O. Box 61098
Raleigh, N.C. 27661
408
p .o.
II
II
II
Banrier Ave.
Box 20328
Greensboro, N.C.
P.O. Box 2728
Hio-h ,0 Point, N.C.
p .o. Box 20926
Greensboro, N.C.
P.O. Box 9601
lreensboro, N.C.
p. 0. Box 3957
Charlotte, N.C.
27420
27261
27420
27408
28203
P .0. Box 3556
Durham, N.C. 22702
II
II
II
II
II
II.
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II.
II
II
,-.-;):·•;_~;-·
::-.::::·:(:(.;
;::<:::•::;=:~:::::;
:l\!!t~~if l-
V~ 0~cf)
~. JJM~.,
•::t,::::::i.;r/·
·-'\i-:{ "'.:~::··-=· -.. ,
'•••,<,•,•,• :/: ---- -
'~¢'<. .~.
.......
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NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT · _,,:. . . . - , ., --.. . . ,, ._p., . ,.,. ~./ L
,. . AIR_ QUALITY SECTION · _:> y,·t,·-(:jit,ii:,.,
{/-·~tt,..,; :,'£.
REQUEST FOR .ACTION TO BE TAKEN
The item'listcd below requires action to ascertain '·complian'ce•undcr Article. 21,
General Statutes of North Carolina,. concerning··rule;,.an'd regulations go;erning· the tion: \ ' · · ·· · ' · · -. ·-· ;,-:-.
Name
Cristex
Subject
SOC followup
I Tl vestigation Requested Hy~
Remarks
Assigned To
ITlvestigated By
'Ron Hawks
Action Recommended
Re-inspect for compliance
Jnvestiption Report
Address
Oxford
Date
2/3/77
·i \ ::.,: i .(
Couuly
Granville
Coullty
D&te
Returned
Contacted Jim Patterson, plant engi~eer and inspected mist eliminate~ installed
on heat set range.
At the time of the inspection the unit was not in operation. The unit.is
complete and is operational, a 55 gallon drum ofcollected water and oil
was collected since start up. ''t
Heat raclaim system and insulation on d~cts have not been completed. Work is
~ontinuing on these items.
A visible emissions was noted from the down stream stack on the second heat set
range. The emission was observed for 15 minutes and exceeded 40% opacity. Further
evaluation of this source is needed to determiile if the emiss_ion is a continuing
problem or a maintenance problem.
Based on the completion of the abatement system the requirements of the SOC have
been met .
Corre·apondence To: -----------------------------··-·------..... _ ---
White;Engin~ering Branch; Yellow-Centra] File;
AQ-16 Rev. 7-1-71
. ;::::-~ ..
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Mr. C. J. O'Bryaut
Cristex Corporation
Industry Drive
Oxford,·llC 27565
Dear !1r. O'Bryant:
September 23, 1977
SUBJECT: Permit Renewal
This letter is to advise you that permit number P-2097 issued
for the operation of air pollution emission sources at your facility
will expire on 12/31/77.
Please advise this office in writing if you wish renewal and
if there are any changes in the·operations covered.under this permit.
If you have installed .new processing equipment or altered the source
in such a manner to·effect your emissions, please request form AQ-22
."Application for A "Permit" To Construct and Operate Air Pollution
Abatement Facilities And/Or Emission· Sources" and submit a revision
with your renewal request.
If I can be of any assistance, please contact me at the below
number.
Sincerely,
rtonald L. lfa.uks
Air Qunl:!.ty Section
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Cristex Corporation, Industry Drive, Oxford, N. Carolina 27565, [phone]
October 17, 1977
Mr. Ronald Hawks
North Carolina Department of Natural Resources
Air Quality Section
P. 0. Box 27687
Raleigh, N. C. 27611
Dear Mr. Hawks:
I am requesting that the Permit No. P-2097 be renewed.
I understand the existing permit expires on December 31, 1977.
There have been no changes or modifications to the
existing equipment covered by the P-2097 permi
JP/mgo
cc: C. J. O'Bryant
John Swift
Jim Patterson
Plant Engineer
Cristex Corp.
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·' ~~-·.: ti /t,,f,.'_L,C/{!_ ~{'
NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT;,..;, , .
AIR QUALITY SECTION 0 /U-'J_.:C:--<j
v:__!l, _ _;,,,_4_£?, :::1 _ z .
REQUEST FOR ACTION TO BE TAKEN cJ. .
The item listed below requires action to ascertain compliance under Article 21, Chapter 143 of the
General Statutes of North Carolina, concerning rules and regulations governing the control of air pollu-
tion:
Name
Cristex
Subject
I!1vestigation Requested By
Remarks
Assigned To
ITlvestigated By
Ron L. Hawks
Action Recommended
Investigation Report
Address
Oxford
Ad<lresS
Date
11/15/77
Counly
Granville
County
Date
Returned
1. Contacted Mr. Patterson concerning permit renewal for mist elliminator on tenter
frame. The unit has not been replaced but. is under construction.
2. Other emission sources are at the site, and I advised Mr. Patterson that these
sources should be covered under the renewed permit. Issued AQ-22's for tenter
frames 2 and 3, boilers and beam dye becks.
3. Re-inspect mist elliminator when in operation and add additional sources.
Correspondence To:
Signature:
White-Engin~ering Branch: Yellow-Central File; Blue-Regional Office
AQ-16 Rev. 7-1-71
, --
------------
I NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT
AIR QUALITY SECTION
I REQUEST FOR ACTION TO BE TAKEN
The item listed below requires action to ascertain compliance under Article
General Statutes of North Carolina, concerning rules and regulations governing I tion:
1 Name
Subject
Cristex
Address
Oxford
I Permit Applications and Permit Renewal
Investigation Requested. By Address
I Remarks
I Assigned To
Iiivestigated By
I , Ron L. Hawks
Action Recommended
I Renew Permit 2097 with Additions
Inveatiption Report
Date
1/19/78
Sft1l.;;•.
'J
21, Chapter 143 of the·
the control of air pollu-
Counly
Granville
. Cou_nty
Date
Returned
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1. Application has been received for operation of two No. 6 oil-fired boilers, two ten-
ter frames, and six beam dyeing tubs.
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2. The dye tubs use several organics for dyeing purposes. In general, the organics
are nonvolat:ili. '.Che dyeing ass is tan ts (carriers) us_ed are ace tic acid/ ace tone,
and are exempt solvents.
3. A napping agent is used on the nylon which causes visible emissions. The use may
result in emissions from tenters 2 and 3 which may exceed 40% opacity.
4. The NCFO recommends issuance of the permit with a visible emission stipulation to
be conducted when the napping agent is being rue..
5. The mist eliminator has been repaired and is in compliance.
I Conupondence To:
I ~ ~..,. : .... ~-··
I Whlte-Enir!neerlnir Branch; Yeitow-Central File; Bhi_e--Reg-!onal Office
AQ-16 Rev •. 7-1-71 · ·.
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NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT
AIR QUALITY SECTION
REQUEST FOR ACTION TO BET AKEN
The item listed below rei1uires action to ascertain compliance under Article
Statutes of North Carolina, concerning rules and regulations governing General 21; Chapter 143 of the
the control of air pollu-tion:
Name
Subject
Cristex
En r. Evaluation
Address
Oxford
Cuunly
Granville
Investigation Requested Hy Address Cou.nty
Remarks
Assigned To Date
Investigated B:, Date
5/23/78
Returned
Ron L. Hawks 6/5/78
Action Recommended
~end notice of violation
Inveatiption Report
1. Observed visible emission from heat set range No. 2 and conducted evaluation. The
range was observed in violation of visible emission standard.
2. The range was processing nylon knit which had been padded with a mineral oil
based napping agent.
3. Advised Mr. Jim Patterson that the furnace was being operated in violation of
the·•;,risible emission standard and that a notii:e of violation would be mailed.
I Correapondence To: --------------------------------------
I
I Whlte-Engineerln11: .Branch; Yollow-Centrtil FIia; .Bluo-Rogioriol Office
AQ-16 Rev •. 7-1-71 ·
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DEPARTMENT OF NATURAL AND ECONOMIC RESOURCES
DIVISION OF ENVIRONOMENTAL MANAGEMENT
Plume Observation Record Form
Date J;/:B/78
Observer ~, J/u?;/,z_
' Checked By _______ _
Type of installation. __ _
Au±-4-d!:,a<Cd'V.;--<,
Fuel '!4.4-Stack Ht. 35 ~.
Observers Distance from Stack
,3() 0 Ft.
Wind Speed ,?-..5 Direct;1.E_
Sky Condition C /Jab-
Pl ume Color 6-,,,J;q
Plume Background A/id-::
Start Time (I : S <2
Ending Time /;? ; 2,(?
Ending Weather
Wind Speed.?-f DirectSE
Sky Condition tCJ./t; 4&
No. Units in Excess of
standard / ,:l_ t/:
5 min/hr. allow 20
No. Units of VIO. / 0 ';/-
Remarks: ---------LiJk /eda,,-f-:
AQ-23 5/26/75
'
~ Mi n
0 lf'O
l /00
2 '?'ti
3 85
4 7.c
5 "J'S
6 95
7 1'7 t'
8 57'0
9 S-.. !/
10 95
11 '>ti
12 'RO
13 CJo
14 ,:;,-/')
15 '9-S'"
16 i;:;"6
17 Ix>,;-
18 7c
19 ,;;,o
20 ~.c;
21 70
22 "1;;
23 'n t;
24 I.I!
25 a--r-
26 "7A
' ' ,; c;~ '77o _i , r.
'28' t;10'
29 'irr7
Address
,s OA AS
'€-3 9CJ 95
5"tl 7{} '83
'70 :;.:,;-'B'CJ
70 75 :,,o
/tlo /0' 75
'?ti 9o 7'0
85 .,;,O 8£:
95 :"CJ ss
85" :;;,,; 70
'DCJ fT..5 9c
'Jo '><CJ "". ;;-
;7§ '5i',".I ',</';
'70 ff'..5 'ff?,
7'.'1 90 7-r,
·"t?J""; s;--o >J'"...!i
90 qq '3c:r
71() ?fO lqo
f?/) e-o ')..5
7C' l7i? 7_.J,
\~,; 9:,.., «c
l-9-tl I /JG 7S
'7'.S 1->6' 1-J.,.,
'7() "/t;' 1"/)
'76 .y,, l'";/i
t.S 70 'irO
9o '70 '9.§
4_r:' 'R'O «ll
7,J:' ,W; \'1$
~/)
' ~ ;,
~{T '?O
*o 71D ?(t;
~ .,,_
•A
,,
..
33
34
3,;
36
37
38
,a
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
I) , ,; ,,., .,,
-2-
Use Gircle to draw a diagram showing any pertinant buildings, trees,
roads etc. in relationship to your point of observation of the source.
,,,JPi
.l...t,i,,,-_/b--"
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-3-
Subtract your positive observational error (P.O.E.), from the
Equivalent Opacity of the readings that are inexcess of the standard
and insert into the proper occurring time frame.
Number of readings of
each colume that exceed
the standard •••••••••••
A. ____ _
B
C
D
E
F
G
H
Number of readings
exceeding standard
Minus 5 min/hr.
allowance ....
Total number of
readings in VIO.
20
----
A
~-Min. 0
0
1
2
3
4
5
,:;
7
8
0
,,,
71
l?
,,
l ,J
"' ,~
17
18
19
20
21
22
23
24
25-
;; o\ : "'· "•26' ;: •• _.:,;
·, ~-..
.'i, ')"'7 ,I )1 ,,.,
OD
29
.TOTAL
B C D E F G
15 30 45 ~ Min. 0 15 30
30
31
32
33
0A
,,,
?£
n
?O
,-
,~
A>
A?
I A?
'
,,
,, .
I ,,
I ·-
I /IQ
49
I Sn
.,
S?
.,
' 54
·~ .. • • ·1 ' ' \J ' ;. I, •~ u ' 1' •' ., :
'?.J ; ~ .. ., ) , M
I ro
59
TOTAL
H
45
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NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT
AIR QUALITY SECTION
REQUEST FOR ACTION TO BE TAKEN
The item listc<l below rei1uircs action to ascertain .compliance under Article
Statutes of North Carolina, concerning rules and regulations governing I General
tion: .
I Name Cristex Corp.
Subject
Renewal and Revision I Investigation Requested Jly
C. J. O'B ant I Remarks
Address
of Permit 1fr2097
Ad<lrf!ss
Conduct Review and Make Reconnnendations
Oxford
21; Chapter 143 of the
the control of air pollu-
County
Granville
Cou_nty
Date I Assigned To Plans Review 1/11/78
Date Returned ITiveatigated By IA --c-ti-on_R_ec_o_mmen-----:-dod..:B..:i::1::1:.....:P..:e..:a::r..:c..:e __ .....:.7:../.:1.:.8.:../:..7.:.8 ________________________ _
II Issue revised permit #2097R and send notice of ~iolation and denial fpr frame
U lnveatlptlon Report 1fr2
Permit #2097 was originally issued for a fiberglass mesh pad type mist eliminator installec
on tenter frame (No. 1).
Cristex has requested renewal by letter dated 10/17/77 and indicates the facility
is as originally specified in the Permit application.
3. Application was received for operation of two 1fr6 oil-fired boilers, two tenter m frames, and six beam dyeing tubs.
4.
m 5.
The boiler emits (.042 lb S02/lb Fuel)/(.019 million BTU/lb Fuel) = 2.2 lb so 2/
million BTU.
The dye tubs use several organics for dyeing purposes. In general, the organics are
nonvolatile. The dyeing assistants are exempt solvents (acid/acetone).
NESHAPS, NSPS, and PSD do not apply.
NSR does not apply (source is existing).
(over)
I Correapondence To:
I -. ':;• .. ,,.,~ ,.
I Whfte-Enirfneerlng-Branch; Yellow-Central File; Blu_•Regional Office
AQ-16 Rev. 7-1-71 ·
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CERTIFIED MAIL
RETURN RECEIPT REQUESTED July 24, 1978
Mr, .C. J. O'Bryant
Exec. Vice President
Cristex-Corporation
· Industry Drive .
Oxford, North Carolina 27565
Dear Mr, O'Bryant:
Reference is made to your application to.operate tenter frames
#2 .and #3. located· at Cristex Corp., Industry Drive, Oxford, North
Carolina, Granville County.
An evaluation of your facilities conducted May 23, 1978 revealed
that tenter frane No. 2 was operating in violation of North Carolina·
.Division of Environmental Management Standard 15 NCAC 2D .0521, "Control
of Visible Emissions."
Consequently, your application for a Permit for ten·ter frame No. 2
is denied. (A _Permit covering frame No, 3 will _be mailed under separate
cover).
This office will be. happy to consider a new a,;.ended application
that proposes a control scheme for visible emissions from frame No. 2
'Which w:>uld demonstrate sufficient control efficiency to comply with
applicable standards.
If there are any questions regarding this matter, feel free to contact
Mr.-Bill Pearce of this office at [phone].·
----
WRP/el
RRO/Rackley
Sincerely,
HOL-_,., "· ,.-: -c;.,.,,.ff ...._ .•.• ,,.. -···-~·--·~-~ LiJi;l
> A:''. F\fcMckoi-1e, Director.
Division·of Environmental Management
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·Mr. Jim Petterson
Plant Engineer
Cristex Corporation
Industry Drive ,
Oxford, North Caroline
Dear Mr. Petterson:
27565
July 28, 1978
Subject: Permit No. 2097R
·cristex Corporation
.Industry Drive
Oxford, :North Carolina
In accordance with your application received January 11, 1978,
· we are forwarding herewith Permit No. 2097R to .Cristex Corporation,
Industry Drive, Oxford, North·Carolina for the operation of (1) six
atmospre ric dye tubs ( processing 1,800 ·pounds per· hour nylon/
acetate cloth each (2) two No. 6 oil-fired boilers (25 x 106 BTU per
hour heat input each) (3) a tenter frame (No. 3) ·and an afr cleaning
device consisting of a fiberglass mesh pad type mist eliminator (360
square feet of face area) and appurtenances installed on tenter frame
·(No. 1) to remove particulate and visible emissions, and for the
discharge of the treated ·air. and associated vent and stackgases into
the outdoor atmosphere at its facility located at Industry-Drive,
Oxford, North Carolina, Granville County.
This Permit shall be effective from the date of its is~uance until
October 1, 1981, is nontransferable to future owners and operators·, and
shall be subject to the conditions and limitations as specified therein.
Enclosure
• . ,
Sincerely,
Or,;,;,,,,i Si.a1ned oy
A. F. McRORIE
A. F. McRorie, Director
Division of Environmental ~anagement
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NORTH CMOLINA
ENVIRONMENTAL MANAGEMENT CO.HI-USSION
DEPARTMENT OF NATURAL RESOURCES & COMMUNITY Dl:."VELOPMENT
Raleigh
For the Discharge of Air.Contaminants.Into the Atmosphere
In accordance with the provisions of Article 21B of Chapter 143, General Statutes
of North Carolina as amended, and other applicable Laws, Rules and Regulations,
PERMISSION IS HEREBY GRANTED TO
Cristex Corp.
IndustrY Drive
Oxford, Uortb Carolina
FOR THE
operation of,
(1) Si:< atJ:lospheric dye tubs · (proce<1s,ing 1, 8v0 pounds per hour nylon/
acetate cloth each)
(2) Two Ilo. 6 oil-fired boilers (:?5 x .106 BTU per hour he'!-t input each)
(3) A tenter frame (No. 3)
and w1 air cleaning device consisting of a fiberglass mesh pad type. mist el:irri.nator
(360 square feet of face area) and appurtenances installed on.tenter frame
(110. 1) to remove particulata·and visible emissions, and for the discharge of the
treated air and associated vent and stackgases into t.~e outdoor atmosphere at
its facility located at. Industry Drive, 0-..:ford, llorth carolina, Granville
County,
in accordance with the application received January 11, 197!>, and in conformity
with the plans, specifications, and other supporting data, all of which are filed
with the De1>artment of Natural Resources & COIJ1nunity Developuient and are incorporated
as part of this Permit.
This Permit shall be effective from tho date of its issuance until October 1,
.1981, is nontransferable to future owners and operators, and shall be subject to the
following spocified·conditions and limitations,
1.
2.
Tile.facilities shall be properly operated and maintained at all times in such a
r.ia.mor as •to effoct an overall reduction in air pollution· in keeping with the
application and otherwise to reduce air contamination to the extent necessary to
comply with applicable EnvirolllllOntal Hanagemant Commission Regulations, including
15 NCAC 2D .0515, .0516, .0518 and .0521.
~ .., " ... ,. .. 1~ ,,::•""t;, •
f ~ t fl ~ , /! I , ........ r~ '\ .•
Report9 on the operation and-maintenance of the facilities shall·be submitted to
the Division of EnviroM,mtal •Mana.gomen't at ·'such interv!'ls and i~ such form and
detail as may be required ·1:,y . the Di vision. Information required in suc.h reports
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Ponui t !lo. 1097R
Page 2
3.
nay include, but is not limited to, process weight rates, firing rates, hours of
operation, and preventive rnninten=co schedules.
A violation of any term or con<lition of th.is Permit. shall subject the Permittee to
enforcement procedures contained in North Carolina General Statutes 143-215.114,
including assessment of civil penalties •.
Permit issued this the 26th day of July,. 1976.
NORTH CAROLINA l:."lNIROIIMENTAL MANAGEMENT COMMISSION
.Permit no. 2097R
l):i:,i:d S,1:1ed DYi
f... JL McRORlE
A. F. McRorie, Director
Division of llnviroru:10ntal Managenent
By Authority of the Secretary of the Dl.lpartment
of natural Resources G Community Development
-' 't'" !·" _.-~;, ~~ ,ti .. :.~ ': ~
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NORTH CAROLI NA
BOARD OF WATER AND AIR RESOURCES
RALEIGH
APPLICATION FOR APPROVAL OF
PLANS AND ISSUANCE OF
A 11PERMIT"
TO CONSTRUCT AND OPERATE AIR
POLLUTION ABATEMENT FACILITIES MD/OR EMISSION SOURCES
Filed By : _.>-Cc:.111-'Iu~J.' J.TJ;EX.,.,___1(.,_,;o_,_· .... ,3_._P~-~---
( Name)
INDUST:1Y D1UV_~E~--
(Address)
OXFORD, N C
I AQ-22 Rev. 8/72
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APPLICATION FOR A "PERMIT"
To Construct and Operate Air Pollution Abatement Facilities and/or Emission Sources
Three Copies to be Submitted
Fourth Copy Should be Retained by Applicant
Date: --"lae-:...),.;-c..7-'-'8"------
I In accordance with the provisions of Article 21 of Ch_apter 143, General Statutes of North Carolina as amended, application
is hereby made by =--,...',!,-J-"-'-' ....... 4!-'..,_.l,'!--!-'-,JW-l--"-'Cls,,...J..l.L-'J-~=~~~-~--~--~--~=---~~ Include Division or Plant Name in Addition ta Parent I · · in the County of r, RA 1'1VT Ji ,T, E . at -dl..Nill.L::..;t:.J~-l1"1;.JLl!;,.,..,-U.l'.!c4..!;ll.l,.._jL._.;...~~~ ~Co_m_p_a-ny_i_f_A~p_p_l_i-ca_b_l_e~) Street and City or own ddress of at or ac1lity
for issuanc,.e of a "Pennit" to construct and operate air pollution abatement facilities and/or emissions sources at above I locatioll as s~ecified in the accompanying drawings, specifications, and other pertinent data:
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1. Nature of Operation Conducted at the Above Facility: TEXTILE KNITTING, DYEING, &: FINISH
3.
Description of Process(es) Whose Emission(s) is/are to be Controlied by the Facility or Source{s) Which is/are to be
Constructed or Altered. (Complete Section I) BOILER ( 2 )?
Furnish Type and Narrative Description of Proposed Control o'evice(s).(Complete Appropriate Supplemental Data Sheets for
Control Device to be Installed and/or Operated. Include Make and Model Number of Control Device(s) and Number of
Identical Units}.
4. Contaminant
Emitted:
Weight Rate of Emissions (lb/hr):
Without ·control Device With Control Device
Co,1trol Efficiency (%}:
Without Control Device With Control Device
I 5. Name and Address of Engineering Firm that Prepared Plans: Manufactor of Boiler-Cleaver Brooks
6. Ultimate Disposition of Collected Pollutants:
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8. Indicate ,Period of Time for Which Facilities
are Estimated to be Adequate: __ Years
I Name:
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(Responsible lndiv1dual of Company Purchasing/
Operating Facility ... PLEASE PRINT)
I Signature and Title:
I AQ-22
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7. Date on .,hich Facilities are to be Completed ·and in Operation:
____ N_A ____ , 19 __ _
9. Estimate Cost of Air Pollution Control Device$ ______ _
10. Hours Facility is Operated Per Year:
Mailing Address: CRISTEX CO~P.
INDUSTRY DRIVE
OXFORD N.C.
Telephone Number: 9] q-69]-6] l1)
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I. GENERAL DATA FOR PROCESSES
• Attach d<t,u.ted pitocM• e.ng-ine£1W1g ,i,u,w,ing•, <4u.lf"'ent dfuwc"8• o.nd 6low cuo.gJIJlmJ, 6o-t .the pitOcM• ( M 1 M •ow,u I• I
be-ing con.t,w.e,ted OJI. a.UM.ed.
Name o·f Process: _...;Peo1.01..iw.J..1ea-r.c;.._ft..t..owrc......1P_~=o"c'-'-"e'-'s"-"s~Scut~e=aumu... __ _
Total Weight of Materials Entering this Process: ____ lb/hr or ton/hr
Volume and Temperature of Air Flow Entering Control Device: CFM@ ---=•F
I Volume and Temperature of Effluent at Discharge Point to Atm-o-sp_h_e_r_e_:_ CFM@ ____ "F
Pollutant(s) tc be Controlled: Inside area of Stack ----~ft2. Height of Process Stack or Vent Above Ground Level _____ ft.
______ lb/hr II Particulate Emission Rate (Before Control)
Particle Size Distribution: 0-5p __ ..,%,, 5-lOp~. 10-20p__J, 20·30p__J, 30-4Dp____l, 4D-50p____l,>5D~____l
D Gaseous Emission(s): Name {Chemical Formula} or 1 b/hr
E II. SUPPLEMENTARY DATA FOR INCINERATORS ·(Including .Conical Incinerators)
I Circle Type of Waste or Indicate Composition: Type 0
Combustible: ___ % Nan-Combustible: ___ % Moisture: ___ % Heat Value: ___ BTU/lb
Type I Type II Type III Type IV
I Total Waste Generated Per Oay: ___ lb.·
Design Capacity for Above Waste: ____ lbs/hr
Hours Incinerator will be Operated: ____ hrs/day
Manufacturer and Model Number; Approximate Cost:
I Primary Chamber Volume: ___ ft.3 .secondary Chamber Volume: ft.3 ---
Total Excess Air __ % Draft: Natural
I Air Requirements:
Overfire Air: cfm Underfire Air: cfm
Is there an Electronically Controlled, Exhaust.Gas Temi,eratu"reModulated, Damper Installed on the
Induced Other
Coni_cal Incinerator for: Overfire Air Supply __ , Underfire Air Supply __ , Dome __ Temperature Set Point
Flame Port Temperature: ___ °F Secondary Chamber Temperatu_re: ___ "F
Is there a Continuous Exhaust Gas Temperature· Recorder? Yes No
Stack: Inside Area __ ft.2 Height __ ft. Gas Velocity __ ft/sec Temperature __ °F Fan Capacity_· _cfm Stack Lined? ___ _
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I Is there a Wet Scrubber?
Yes No 1· Aux. Fuel: Oil
Flow Rate of H20 into Scrubber __gal/min Temperature Before Scrubber __ "F
Gas Other
'
Burner Rating: Primary Chamber
---~BTU/hr
No Preheating Time:
Secondary Chamber
----'BTU/hr
----'min.
Stack
__ BTU/hr
I Primary Burner: Is there a Preheat Timer? Yes
Secondary Burner or Afterburner: Is there a Timer? Yes No length of Time Burner is Operated ___ min.
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Is the Timer Reset by Charging Door? Yes No Other Mode of Burner Control
Type of Feed: Manual Automatic If Automatic, Describe----'------------------
Distance from Incinerator to Nearest Structure(s) in which People Live and/or Work. ___ ft.
Signature:
d .,.;,
•
Title:
r,: .. ,,.,"' "
t: .-,~•--2. ,;
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Ill. SUPPLEMEITTARY DATA FOR FUEL BURNING SOURCES
I •Attach dwul.ed d.iJne.w,.i.oned ~ OIi. •kmh •ho1<1<ng .i.n.l:'11.n.oi. 6'1ttWl.u 06 dluJ=, wool OIi. coal. 6.U..ed bo.il.'11.4, and
1tec.ov Vtt.J boi.lelt.6 • ·
Type of Fuel Burning Source _ __._B,,_o,._i ...... l..,e._rL..._..J(w?'-..L) __ I Make and Model Number Cleaver Brooks 6OOH:ij'olume of Furnace
Stack Height Above Ground Level _lift.
ft3
Inside Area of Stack 2J2b.. ft2
I Specify Actual Amount of Each Fuel Used in Above Source (s):
Coal lb/hr; Oil Grade _jj_6_ Amount 1.6.1. gal/hr, at __ BTU/gal and __ lb/gal or lb/hr
I Wood lb/hr; Natural Gas2SM SCF/hr, at BTU/SCF; Other ___________________ _
·(Specify type, amount and heating value)
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Specify Maximum Rating for Each Fuel Burning Sou.rce:
Coal on #6 Wood Natural Gas X Other __________________ _
Maximum. Sulfur Content of Fuel 2-.a...l %
Type of Solid Fuel Burning Equipment Used:
Specify Standby Fuel _}j_Q_ Maximum% Sulfur ~l
Hand Fired Spreader Stoker Underfeed Stiker Chain Grate
Traveling Grate Pulverizer_ Cyclone Fu_rnace _ Other (Specify) ______ _
Ash Content of Fuel: Specify Method and Schedule of Tube .. Cleaning, if Applicable:
Coal I Wood % Other Lancing _____ _ Tube Blowing ______ Schedule ______ _
Emission Control Equipment (Describe in Detail in Sections IV an~ V)
Collection Device:· Wet __ Dry__ Steam Injection Air Injection __ Is Collected Flyash Reinjected?
-Oraft on Beile~ (Natural Induced ) · cfm at Of
Total Number of Fuel Burning Sources Within Property iourid'aries: ~
Maximum Capacity Rating, by Type, for All Fuel Burning Units Excluding that Itemized Above: (Total Like Units)
Coal 1 b/hr Wood lb/hr Oil __ gal/hr Natural Gas __ SCF/hr
IV. SUPPLEMENTARY. DATA FOR WET COLLECTION DEVICES
•A:tta.ch de,,ta,il.ed engine.VUJ'lg dlt.aw.utg~ 06 the. cont:ltol. de.vice. a.nd paltUcle. .oize. vvu.u..6 1t.emoval e.66,.i.C-<.e.nc.y c.u1tvu.
Liquid Scrubbing Medium and Additives: -Total Liquid Injection Rate (Include Recirculated and Make-up Rates) __ gal/min or gal/1000 ft3
Operating Pressure Drop Across Device __ in H20
ANSWER FOLLOWING QUESTIONS FOR SPECIFIC DEVICE:
VENTURI SCURBBER: Inlet Area in2 Throat Area in2 Throat Velocity __ ft/sec
GRAVITY SPRAY CHAMBER: Number of Nozzles Liquid Droplet Size __ u Co-Current Countercurrent
WET CYCLONE: PACKED TOWER DR PLATE TOWER:
Body Diameter in Length in Cross-Sectional Area _____ ft2 Type of Plate ______ _
Inlet Area in2 Number of Nozzles Length ___________ ft Depth of Packing _____ _
Outlet Area in2 Number of Plates Type of Packing _____ _
OTHER WET COLLECTION DEVICES: GIVE COMPLETE DESCRIPTION INCLUDING DESIGN PARAMETER~D DETAILED ENGINEERING DRAWINGS. r r.J ·n r " ~-•·"':, :·: ,l .~:-!')'~." I -i..:: ;-~·~-~t 1° ·.1 1 rA.··;·e = -· ·, :_ '.. \r
------------"".'-.-~:..: ~··:~-.. -. -"---'--~~.-' ~'--'--'"'---"-'---'--------------Signature:
- 3
V. SUPPLEMENTARY DATA FOR DRY COLLECTION DEVICES
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BAGHOUSES: Cloth Area ____ ft2
•At..t.a.c.h de.ta.i..l.ed eng-Ote.£/Ung dltaw.utgo 06 .the cont.to! de.v.ic.e a.nd pa:t..ti.cl.e. 6..i.ze. Ve/ULUI Jte.mova.l. e.66,icie.ncy CLJ.ltve,L
Bag Ma teri a 1
I Number of Compar~nts _______ _
Method of Cleaning ________ _
Pressure~ Drop Total in H20
Air-to-Cloth Ratio ft/min ---------
Time Between Cleaning
I ELECTROSTATIC PRECIPITATORS:
mins, hrs
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GENERAL:
___ ft2 Effective Area of Grounded Collector Plates
Number of Compartments or Chambers Number of Cells per Compartment _____ _
Electrical Field Gradient at the Discharge or Emitting Electrodes _____ KV/in
Average Electrical Field Gradient at the the Grounded Collecting Electrodes _____ KV/in
Fields of Treatment ____ Potential Applied to Emitting Wires ___ KV
SINGLE STAGE TYPE:
Distance Between Emitting Wire~ and Collecting Plates _____ in.
Number of Isolatable Bus Sections _____ Corona Power ____ Watt•/1000 cfm
TWO STAGE TYPE:
Distance Between First Stage Emitting E-lectrodes and Field Receiver Electrodes {Ground) ____ ·in
Potential Applied to Second Stage Emitting Plates _____ KV
Distance Between Second Stage Emitting Plates and Grounded Collection Plates _____ in
I) CYCLDNES/MUL TICYCLONES:
IJ Simple Cyclone Multicyclone
Diameter __________ _ in Diameter in
Inlet Dimensions ______ _ Inlet Dimensions of Individual Cyclone
Outlet Dimensions-~'------Outlet Dimensions of Individual Cyclone
Pressure Drop ______ _ in H20 Pressure Drop in H20
Number of Cyclones ______ _ Number of Cyclones
1· OTHER DRY COLLECTION DEVICES: GIVE COMPLETE DETAILED ENGINEERING DESCRIPTION AND DRAWINGS.
1 Signature: Title:
-4 -I
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I l,c,s ;-"S
,-:, .. , •·~
Jr.,. .. ·",;
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··-··~ ...• /
-- --I!!!! I!!!!!
VI. AREA DIAGRAM
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i== . liiiiiii liiii iiii - -().;ner __ LC~TC?iT!.;:i'sc.:!'P.:.JEo:.· &(JC.i•'\l..!JTC?.::01.()L:"1:W.11 .::"':cIL!.O.J.i>!"?-J_.~---
. Location H!DUS'l'"1Y n:-i VE, QXF:J'?D, N,C.
Give Street ddress
INSTRUCTIONS:
1. Show all surrounding buildings and roads within
1000 feet of subject equipment which is located
at center of circles.
2. Indicate location and type of building by the
use of small numbered circles with the de-
scription below.
-3. Show roads as 11nes representing the road edges,
Indicate.street names and highway numbers ..
4. Show wooded or cleared areas by approxi"m.1te
boundary lines and.the words 11woods". .. cleared".
11cornfield". etc.
5. Indicate direction of north by arrow.·
CODE DESCRIPTION
G)
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EXAMPLE
Cristex Corporation
Office
. Boil er Room
G) Church
@ Residence
, X Indicates locatioO of equipment.
. Gristex Corporation
" Industry Drive ·
Oxford, N. Carolina 27565
&~(?)
l!l!!!!!I I!!!!!! !!!!!!
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NORTH CAROLI NA
BOARD OF WATER AND AIR RESOURCES
RALEIGH
l'Jr lit_['(} 1 , _
.._, I " r, , -._ .. ·: ; \/ 7 . ,I · · -1 1978
APPLICATION FOR APPROVAL OF
PLANS ANO ISSUANCE OF
A "PERMIT"
TO CONSTRUCT ANO OPERATE AIR
POLLUT!Oil ABATEMENT FACILITIES AIIO/OR EMISSION SOURCES
Filed By: crnsTg( CQ 131'.
(Name)
INDlJS'l':lY D:lIV."-'E=-·-· __
(Address)
_Q.XJcQJID1.,,~~"-I ....c,C ____ _
AQ-22 Rev. B/72
~.,,,, .. ., ~,: 'f,.,. ~ j .. -.,.
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APPLICATION FOR A "PERMIT"
To Construct and Operate Air Pollution Abatement Facilities and/or Emission Sources
Three Copies to be Submitted
Fourth Copy Should be Retained by Applicant
Date: 1-5-78
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, application
is hereby made by CRISTElC CORPORATION
(Name of Company, Establishment, Town, Etc.) {Include Division or Plant Name in Addition to Parent
==C.,.-C'7"C~==~in the county of '1l'lA'l'fI11E at INDUSTRY DTTIVE, OXFORD, N.C. Company if Applicable) (Street and City or Town Address of Plant or Facility)
for issuance of a "Permit11 to construct and operate air pollution abatement facilities and/or emissions sources at above
location as specified in the accompanying drawings, specifications, and other pertinent data:
1. Nature of Operation Conducted at the Above Facility: TEXTILE KNITTING, DYEING, & FINISHIN'.x
2. Description of Process(es) Whose Emission(s) is/are to be Controlled by the Facility or Source(s) Which is/are to be
Cons true ted or Altered. (_Comp 1 ete Section I)
TENTER FRAMES #2 and #3
3. Furnish Type and Narrative Description of Proposed Control Device(s).(Complete Appropriate Supplemental Data Sheets for
Control Device· to be 1nstalled and/or Operated. Include Make and Model Number of Control Device(s) and Number of
Identical Units).
NONE
4. Contaminant
Emitted:
Weight Rate of Emissions (lb/hr): Co,1trol Efficiency (%):
Without Control Device With Control Device Without Control Device With Control Device
5.
VISIBLE
EiUSSIONS
Na~e and Address of Engineering Firm that Prepared 'fi-2 McCreary Machine Works
6. Ultimat~'o{1~0~18ti'on~t' 'loilected Pollutants:
8. Indicate Period of Time for Which Facilities
are Estimated to be Adequate: __ Years
Plans: #3 Vanvlaandern Machine Co.
. Paterson N.J.., 7. Date on Which Facr11t1es a~e to be ~ompleted and in Operation:
--------· 19 __
9. Estimate Cost of Air Pollution Control Device$ _____ _
10. Hours Facility is Operated Per Year:
Name:
(Responsible Individual of Company Purchasing/
Operating Facility ... PLEASE PRINT)
Signature and Title:
AQ-22
Mailing Address: CRIS'I'EX COR?ORATION
INDUSTRY DRIVE
QXEQRD, N.C 27565
Telephone Number: 919-693-6141
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I. GENERAL DATA FDR PROCESSES
*At:to..ch de..tLLU'.ed p1tocu.6 enginec-Ung dJtlwJingJ, equi..p11i"en.t dlt.awing-6 a.nd 6tow dia.g1t.am6 6011. :t.he p:toc.e.b&{e.o) OIL JOU/1.c.e{.til
be.i.ttg c.otUitwcte.d Olt. o...lt.eJle.d..
Name of Process: Tenter Frames #2 and #3
Total Weight of Materials Entering this Process: 2800 1 b/hr or ton/hr
Volume and Temperature of Air Flow Entering Control Device: 14450
Volume and Temperature of Effluent at Discharge Point to Atmosphere:
CFM @
Nylon/Acetate Cloth
290 °F
Pollutant(s) tc be Controlled: Visible Emissions
Height of Process Stack or Vent Above Ground Level __ _.2_~..,__ ft.
Particulate Emission Rate (Before Control) _______ lb/hr
____ __:CFM@ ----°F
Inside area of Stack lJ,2 ft2.
Particle Size Distribution: D-5p_____;, 5-1Dp __ %, 1D-2Dµ______l, 2D-3Dp______l, 3D-4Dp______l, 4D-5Dp______l,>5D~______l
Gaseous Emission(s): Name (Chemical Formula} or lb/hr
II. SUPPLEMENTARY DATA FDR INCINERATORS (Including Conical Incinerators)
Circle Type of Waste or Indicate Composition: Type D Type Type II Type 111 Type IV
Combustible: ___ % Non-Combustible: % Moisture: ___ % Heat Value: ___ BTU/lb
Total Waste Generated Per Day: ___ lb. Hours Incinerator will be Operated: ____ hrs/day
Design Capacity for Above Waste: ____ lbs/hr Manufacturer and Model Number; Approximate Cost:
Primary Chamber Volume: ft.3 Secondary Chamber Volume: ft. 3
Air Requirements: Total Excess Air __ % Draft: Natural Induced Other
Overfire Air: __ cfm Underfire Air: cfm
Is there an Electronically Controlled. Exhaust Gas Temperatu'reModulated, Damper Installed on the
Conical Incinerator for: Overfire
Flame Port Temperature: °F
ls there a Continuou~ust Gas
Stack:
Inside Area __ ft.2 Height __ ft.
Air Supply __ , Underfire Air Supply __ , Dome ___ Temperature Set Point
secondary Chamber Temperature: ___ °F
Temperature Recorder? Yes No
Gas Velocity __ ft/sec Temperature __ °F Fan Capacity __ cfm Stack Lined?
IJ Is there a Wet Scrubber?
Yes No Flow Rate of Hz° into Scrubber _· __ gal/min Temperature Before Scrubber °F
Aux. Fuel: Oil Gas Other
Primary Burner: Is there a Preheat Timer? Yes
Burner Rating: Primary Chamber
____ BTU/hr
Secondary Chamber
_____ BTU/hr
No Preheating Time: ___ _:min.
Stack
__ BTU/hr
Secondary Burner or Afterburner: Is there a Timer? Yes No length of Time Burner is Operated ___ min.
Is the Timer Reset by Charging Door? Yes No Other Mode of Burner Control _________ _
Type of Feed: Manual Automatic If Automatic, Describe ____________________ _
I Distance from Incinerator to Nearest Structure{s) in which People Live and/or Work. ___ ft.
Title: _____________________ _
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Ill. SUPPLEMENTARY DATA FOR FUEL BURNING SOURCES
'Atta.ch de,ta,.Ue.d fue.n.1ii..one.d dJz.a.w.ing 011.. .1iketc.h .t.howi..ng intvuuz.l 6 ea.t.u.Jtu o 6 d//.ye:u,, wood OIL c.oal. 6i.Aed. boilvu.,, a.nd 11..ec.ovvq; boile,'1..6.
#2 and #3
Typ_e of Fuel Burning Source ..T.en.ter Frames Stack Height Above Ground Level .2.5_ ft. Inside Area of Stack 1.J......2ft2
VanVlnandern #J
Make and Model Number McCreary #2 and. Volume 1Jf Furnace ft3
Specify Actual Amount of Each Fuel Used in Above Source {s):
Coal lb/hr; Oil Grade Amount gal/hr, at BTU/gal and lb/gal or lb/hr
Wood lb/hr; Natural Gas 6..QQ_()SCF/hr, at l..Q4DBTU/SCF; Other ___________________ _
(Speclfy type, amount and heating value)
Specify Maximum Rating for Each Fuel Burning Source:
SCF'/hr.
Coal Oil Wood Natural GaslO, 000 Other --------------
Maximum Sulfur Content of Fuel % Specify Standby Fuel Maximum% Sulfur
Type of Solid Fuel Burning Equipment Used: Hand Fired Spreader Stoker_ Unct'erfeed St.')ker _ Chain Grate
Traveling Grate_ Pulverizer_ Cyclone Furnace_ Other (Specify) ______ _
Ash Content of Fuel: Specify Method and Schedule of Tube Cleaning, if Applicable:
Coal % Wood % Other % Lancing _____ _ Tube Blowing ______ Schedule _____ _ II Emission Control Equipment (Describe in Detail in Sections IV and V)
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Collection Device: Wet __ Dry__ Steam Injection
Draft on Boiler (Natural Induced cfm at
Total Number of Fuel Burning SourceS Within Property Boundaries:
Air Injection
Of =:c
Is Collected Flyash Reinjected?
Maximum Capacity Rating, by Type, for All Fuel Burning Units Excluding that Itemized Above: (Total like Units)
Coal lb/hr Wood lb/hr Oil __ gal/hr Natural Gas __ SCF/hr
IV. SUPPLEMENTARY DATA FOR WET COLLECTION DEVICES I *A.tta.c.h de..ta,de.d e.ng-i.nee,Ung a'ltaw-i.n.gJ 06 the. c.onbwl de.v-i.c.e. a.nd pa.,llic.le. J-i.ze. VVLou.6 1te.mova..t e.66-i.c..-i.enc.y c.:.v·wu.
liquid Scrubbing Medium and Additives:
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Total Liquid Injection Rate (Include Recirculated and Make-up Rates) __ gal/min or gal/1000 ft3
Operating Pressure Drop Across Device __ in H20
ANSWER FOLLOWING QUESTIONS FOR SPECIFIC DEVICE:
VENTURI SCURBBER: Inlet Area in2 Throat Area in2 Throat Velocity ft/sec
GRAVITY SPRAY CHAMBER: Number of Nozzles Liquid Droplet Size __ u Co-Current Countercurrent
WET CYCLONE: PACKED TOWER OR PLATE TOWER:
Body Diameter in Length in Cross-Sectional Area n2 Type of Plate
Inlet Area i n2 Number of Nozzles Length ft Depth of Packing
Outlet Area in2 Number of Plates Type of Packing
OTHER WET COLLECTION DEVICES: GIVE COMPLETE DESCRIPTION INCLUDING DESIGN PARAMETERS AND DETAILED ENGINEERING DRAWINGS.
Signature:
{:r-r·-~-J
---------",---,"----,------.. ..,, ' ~ j,, ~
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V. SUPPLEMENTARY DATA FOR ORY COLLECTION DEVICES
•Atta.ch de,ta...il,ed eng.i.ne.e/Ung d,taW-i.ngo 06 the. conbwl dev,i.c.e. a.nd paJr..tic.le o.i.ze. v~tw 11.emovctt e.66-i.ci.e.nqr cl.Ur.vu.
BAGHOUSES: Cloth Area ____ ft2 Bag Material
Number of Compartments ______ _ Pressure -Drop Total ________ in H20
Method of Cleaning Air-to-Cloth Ratio _________ ft/min
Time Between Cleaning mi ns , hrs
ELECTROSTATIC PRECIPITATORS:
GENERAL:
Effective Area of Grounded Collector Plates
Number of Compartments or Chambers
ft2
Number of Cells per Compartment
Electrical Field Gradient at the Discharge or Emitting Electrodes _____ KV/in
Average Electrical Field Gradient at the the Grounded Collecting Electrodes ____ KV/in
Fields of Treatment _____ Potential Applied to Emitting Wires ____ KV
SINGLE STAGE TYPE:
Distance Between Emitting Wires and Collecting Plates _____ in.
Number of Isolatable Bus Sections _____ Corona Power ____ Watts/1000 cfm
TWO STAGE TYPE:
Distance Between First Stage Emitting Electrodes and Field Receiver Electrodes {Ground) ____ in
Potential Applied to Second Stage Emitting Plates ____ KV
Distance Between Second Stage Emitting Plates and Grounded Collection Plates ____ in
CYCLONES/MULTICYCLONES:
Simple Cyclone Multi eye lone
Diameter _________ _ in Diameter in
Inlet Dimensions Inlet Dimensions of Individual Cyclone
Outlet Dimensions ______ _ Outlet Dimensions of Individual Cyclone
Pressure Drop ______ _ in H20 Pressure Drop in H20
Number of Cyclones ______ _ Number of Cyclones
OTHER ORY COLLECTION DEVICES: GIVE COMPLETE DETAILED ENGINEERING DESCRIPTION ANO DRAWINGS.
Signature: _________________ _ Title:
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VI. AREA DIAGRAM
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---..1000----
----- - -
C>wner C 1n "-'T' EX rn :g 0 Q 'Q 1\ '1'JiJ N
loC:ation 'Ii;;, 0XFQ3I2, N, r;.
INSTRUCTIONS:
1. Show all surrounding buildings and roads within
1000 feet of subject equipment which is located
at center of circles.
2 •. Indicate location and type of building by the
use of small numbered circles with the dt·
scrip~ion_below.
3. Show roads as lines representing the road edges.
Indica.te street names and highway numbers.
4. Show wooded or cieared areas by approximate
boundary lines and the worOs "woods", "cleared",
"cornf1eld0 , etc.
5. Indicate direction of north by arrow.·
CODE
CD
®
G)
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(J)
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@
EXAMPLE
D~SCRIPTION
Cristex Corporation
Off'..:,cs
Boiler Room
CD Church
® Residence
X Indicates location of equipment.
' . .
.·._. _._.,_ ....
.~ ~tex~or2 ;' ! . '. -c-.-, Industry Drive
··: , Oxford, N. Carolina 27565
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CERTIFIED MAIL
. RETURN RECEIPT. REQUESTED
Mr. Jiin Patterson
Plant Engineer
Cristex Corporation
Industry Drive
Oxford, NC 27565
Dear Mr. Patterson:
July 27, 1978
During a ·routine inspection of your. facility on l'.ay 23, 1978, a violation of
the Visible Emission Standard. (15 NCAC 2D · .0521) was observed occurring from the
No. 2 drying oven.
Based on discussions with you and our observations, it appears that this
violation is the direct result of the finishing of nylon fabric.containing a
chemical napping agent.
Under the Post Attainment Policy of the North Carolina Air Quality Regulations,
any source.which is not in compliance with emission standards is required to enter
into a Special Order by Consent which specifies a schedule which will lead to·an
expedient abatement of the emissions, This schedule must contain the following:
date on which a final plan will be filed·for review specifying abatement equipment
or process change, date on which a contract or purchase order will be 1st, date on
whid, construction will begin, and date on which final compliance will be achi.;s;,:,d.
It is requested that you review your operation, contact equipment suppliera,
·notify this office· within thirty (30) days of your intent to comply with the Air-
Quality emission·standards, and specify a date on which we·may meet to discuss an
abatement schedule. · ·
Should you have any q.uestions, please contact me.
. RLH/tja
cc:
Mr.
Mr,
Sincerely,
Ronald L. Hawks
Environmental Engineer
Air Quality Section
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NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT
AIR QUALITY SECTION
REQUEST FOR ACTION TO BE TAKEN I The item listc<l below requires action to ascertain compliance under Article
General Statutes of North Carolina, concerning rules and regulations governing
tion:
21; Chapter 143 of the
the control of air pollu-
• ------------------------------'-c---~•,,..,.· -,-' ;..,";-c;-'-,,,---;;' ~c,-,'~-i-"ic-------Name Add res':\ :·: ·J U l d \ :1 I U County
I Subject
Crixtex
Professional Consultation I Inve~tigation Reque~t.-ed By
Rsm.a.:-lu
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As~ignl!d To
I lnvestig,ted By
Ron Hawks II Action Recommendad
Negotiate time frame for compliance a 1nv .. tiption Ra:90rt
Oxford
A<l<lress
Date
7-28-78
Granville
County
Date
Returned
8-7-78
D 1. Contacted Mr. Patterson to discuss compliance of No. 2 tenter frame with the
visible emission standard.
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2. Mr. Patterson indicates that the plant was considering the expansion of the
mist eliminator on the No. 3 frame with the No. 2 frame to be tied in.
3. Advised him that a permit was required to make the change.
IWhit.e.Znz!ne-erfn_i Br~nc.h: Y~11ow-Centr31 Pila; Blu.~Reg1ori1I Office
AQ-16 Rev •. 7-1-71
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NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT
AIR QUALITY SECTION . ;
REQUEST FOR ACTION TO BET AKEN
The item listed below requires action to ascertain compliance under Article 21, Chapter 143 of the
General Statutes of North Carolina, concerning rules and regulations governing the control of air pollu-
tion:
N.O.V. Letter of Intentions
Investigation Requested Hy
Raleigh Regional Office
Remarks
Assigned To
Raleigh Regional Office
Investigated By
Jerry Clayton, Ron Hawks
Action Recommended
.---··Address --.......
Oxford
'··-··'---------
Address
Date
9 20-78
Await finalization of preposed intentions
Investigation RePort
Count.y
Granvi ,·;-;---....
County
Date
Returned
D 1) Talked with Mr. Jim Patterson, PtT. Engineer concerning corrective action to be taken.
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2) They are preposing a #6 fuel hot oil heater capable of handling exhaust from three frame
with some heat recovery. The plans for this unit are not finalized and a request for
deferral of enforcement is to be sent.
3) Control equipment was down at this time due to a cut water main. Repairs were being
made and equip. was to be back on line within 12 hours.
CorroapGndence To:
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NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT
AIR QUALITY SECTION
REQUEST FOR ACTION TO BE TAKEl'RECf/VfC;
The item listc<l below requires action to ascertain compliance under Article 21,
General Statutes of North Carolina, concerning rules and regulations governing the
tion:
DEC 211q?:i
Chapter 143' of the
control of air pollu-
l rE:.:--P-l=s_Re".~w ~
~:~~-, -J,~--
County
Granville ) ----,/ 1 AQ-22 Review
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Investigation Requested By
Raleigh Regional Office
Remarks
Assigned To
Raeigh Regional Office
Investigated By
Jerry Clayton
Action Recommended
Address
Date
11-29-78
County
Date
Returned
D Issue Permit with reference to S.O.C.
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lnveatlptlon Report
1)
2)
3)
Cristex is presently using this same type of system on tenter frame no. 1 for control
of V. E. with no occurrences of violations.
Control system would appear to be sufficient to handle their emission from tenter frame
no. 2 as this is the same type operation as frame no. 1.
Permit should reflect the compliance steppes and dates listed in the Special Order by
Consent. (
Correapondonce To:
. . ~c .....
Whlte-Enclneertnr Branch; Yellaw-C..ntral Filo; '8luo-Roglonol Office
AQ-16 Rev. 7-1-71
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Cristex Corporation, Industry Drive, Oxford, N. Carolina 27:;if-,5, [phone] e,\'o c::i""'
Ml'.'. Ronaid Hawks
Department of N. C. Natural &
Economic Resources
Box 27687
3800 Barrett Drive
Raleigh, N. C. 27611
NS(;; e,0
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November 22, 1978
t.Jn\/ ·J I"? 1070 ,·,·-·, .:...:. .' 1..., 0
In Re: Violation of i:he Visible Emissions Standard (15 NCAC ZD:0521) on No. 2 Tenter Frame, letter dated July 27, 1978
Dear Mr. Hawks :
After receipt of your letter on July 27, 1978 advising me of i:he Visible Emissions Violation, we began immediately i:o investigate the best possible means to correct this problem.
Because of i:he present economic si:ai:us of this company we feel i:hai: ii: is best ai: this time i:o install only a control device i:o eliminate this problem.
We propose i:o install the same type of system i:hai: is presently operating on i:he No. 1 Tenter Frame. This system will be manufactured by the same company, Piedmont Energy Systems.
This air cleaning device consists of a fiberglass mesh pad type mist eliminator i:o remove i:he particulate and visible emissions from i:he exhaust stacks and discharge i:he treated air i:o i:he outdoor atmos-phere.
A permit application i:o construct and i:o operate this equipment is also enclosed.
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Mr. Hawks Page 2 November 22, 1978
April 2, 1979: Delivery of equipment, begin installation.
June 1, 1979: Installation complete~ begin testing.
June 30, 1979: Performance test -final acceptance complete.
I will be available anytime to discuss this abatement schedule.
JP/bdb
Enclosure
Sincerely, -------CRIS1"X CORPORAT ----------
Jim atterson,
Plant Engineer
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RECEIVED NOV 3 O lQ?q
I NORTH CAROLINA
I .ENVIRONMENTAL MANAGEMENT COMMISSION
RALEIGH
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E APPLICATION FOR
A "PERMIT"
I TO CONSTRUCT ANO OPERATE AIR
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Filed By: CRIS'l'RX CQRP
I (Name)
INDTJST'·lY DP.I'TE
I (Address)
OXFORD, N.C.
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APPLICATION FOR A "PERMIT"
To Construct and Operate Air Pollution Abatement Facilities qnd/or Emission Sources
Three Copies to be Submitted
Fourth Copy Should be Retained by Applicant
Oate:NQl1"1'1"ER 22, J 978
I In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, application
is hereby made by C•USTEX t;QRP.
(Nnme of C~mpany, Establishment, Town, Etc.) {Include Division or Plant-Name in Addition to Parent
m ~-~~--~in the County of GRANVILLE at INDUSTRY DRIVE, OXFORD, N.C. Company if Applicable) (Street and City or Town Address of Plant or Facility)
for issuance of a "Permit" to construct and operate air pollution abatement facilities and/or emissions sources at above n location as specified in the accompanying drawings, specifications, and other pertinent data:
1. Nature. of Operation Conducted at the Above Facility:
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TEXTILE KNITTING, DYEING, & J<INIS\iING
Description of Process(es) Whose Emission(s) is/are to be Contro1ied by the Facility or Sou·rce(s) Which is/are to be
Constructed or Altered. [Complete Section I) 'l'EXTILE T:SN'fER FRAhE # 2
Furnish Type and Na rra ti ve Description of Proposed Contra 1 Device ( s). (Complete Appropriate Supplemental Data Sheets for
Control Device to be Installed and/or Operated. Include Make and Model Number of Control Device(s) and Number of
Identical Units). PACKED J_i-IL-'EER BEJ), !TGT{ EFFICIENCY, HEDIUH PRESSURE DR::JP,
011 ?!Io'.i' CU.uLb,C'l'lON. P l£JJ:1UN'r EN,t;c/lJY Sl'S'i'lsfll.
SAME AS UNI'l' INSTALLED ON #1 TENTER PERi'LTT NO. 2097R
Co,1trol Efficiency (%): Contaminant
[mitted:
Weight Rate of Emissions (lb/hr):
~Ii thout Control Device ·w; th Control Device Without·Control Dex.ice With Control Device
OIL MIST 9 5%
Name and Address of Engineering Firm that Prepared Plans: PIED;IJONT ENERGY SYSTE/1S
100 EAST WILYIN,'.-:-ON. BLVD. BELMONT, ND RTE CAPOLINA 28012
6. Ultimate Disposition of Collected Pollutants: 7. Date on Which Facilities are t~ be Completed and in Operation:
8. Indicate Period of Time for Which Facilities
are Estimated to be Adequate: 2..Q_Years
___,J"--1"'JL"'-Y""'._.,_l ____ • 19 79
9. Estimate Cost of Air Pollution Control Device $ 60,000.
I Name:
10. Hours Facili_ty is Operated Per Year:
r,.J. Cl'BRYf,NT -EXEC. 'l.P. Mailing Address: CRIS'PFX t;Q"lP,
(Responsib1e Individual of Company Purchasing/
6000
Operating Facility ... PLEASE PRINT)
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I. GENERAL DATA FOR PROCESSES
,. , _J • • .1~,..,,;1'"', ,.,., .. :rm·-.. .,. ..1~A .. ,:ng• Q. .. .J 1u-u,. dl.o.g1tam& 1o .. lL the ri11 oc.e.6.6[e.&) 0/t .60uJtc.e{.6) Atta.c.,l de..tlLA.,tw p!I.OC.e.6h eng..(.nec.'U..ng u.r~.....,,,.,_ -:,<> "'"....,,,_,. ... iul,t., r.vu.,.w.1.. <> nu ou, o ,,~
bU.ng c.o~tJtuc...ted Olt a..ltCAed.
I Name of Process:
Total Weight of Materials Entering this Process:
TET-!TER F'lAi1E HQ. 2
3200 lb/hr or ton/hr nYLCN / ACE.TATE CLOTH
Volume and Temperature of Air Flow Entering Control Device: 14025
Volume and Tempera·ture of Effluent at Oisctiarge_ Point t~ Atmosphere:
CFM@ ~1[ "F
] Q/179~ FM @ 100
Po 11 utant (s) tc be Contro 11 ed: _;OeaiuL'--"lc,•iia!a . .,S,,_TL-----------------~----
Ins i de are~ of ~tack lJ. 2 Height of Process Stack or Vent Above Ground
Particulate Emission Rate {Before Control}
Level _,,2cc<:;'+----ft.
11+• i lb/hr
Particle Size Distribution: 0-5p 9 c; %, 5-lop:._s__i;, 10-20p_J, 20-30p___i:, 30-4Dp___i:, 40-50p__i;,>50p___i: II . GaSeous Emission(S): Name ·{Chemical Formula) or lb/hr
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II. SUPPLEMENTARY DATA FOR INCINERATORS (Including Conical Incinerators)
Circle Type of Waste or Indicate Composition: Type 0 Type I Type II Type I II Type IV
Combustible: % Non-Combustible: ___ % Moisture: % Heat Value: · __ BTU/lb
Total Waste Generated Per Oay: ___ lb. Hours Incinerator will be Operated: ___ hrs/day
Design Capacity~for Above ~Jaste: ____ lbs/hr Manufacturer and Model Number; Approximate Cost:
Primary Chamber Volume: SeCondary Chamber 'volume: ft. 3. ---
Air Requirements: Total Excess Air % Draft: Natural Induced Other
Overfire Air: cfm Underfire Air: cfm
Is there an Electronically Controlled, Exhaust Gas Terilperatu'reModulated, Damper tn·stalled on the
Conical Incinerator for: Overfire
Fl°ame Port Temperature: ___ °F
Is there a Continuous Exhaust Gas
Stack:
Inside Area __ ft.2 Height_· _ft.
Air Supply_·_, Underfire Air Supply __ , Dome __ Temperature Set Point
Secondary Chamber Temperature: ___ °F
Temperature Recorder? Yes No
Gas Velocity __ ft/sec Temperature °F Fan Capacity __ cfm Stack Lined?
II Is there a Wet Scrubber?
Yes_ No II Aux. Fuel: Oil
Flow Rate ~f H20 into Scrubber __gal/-~in Temperature Before Scrubber __ °F
Gas Other
II Primary Burner: Is there a Preheat Timer? Yes
Burner Rating: Primary Chamber
____ .BTU/hr
No Preheating Time:
Secondary Chamber
---~BTU/hr
---~min.
Stack
__ BTU/hr
SeCondary Burner or Afterburner: Is there ·a Timer? Yes No Length of Time Burner is Operated ___ min.
ls the Timer Reset by Charging Door? Yes No Other Mode of Burner Control
Type of Feed: Manual Automatic If Automatic, Describe
I Distance. from Incinerator to Nearest Structure(s) in whicti
Signature: Title:
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Ill. SUPPLEMENTARY DATA FOR FUEL BURNING SOURCES
• Atta.di de..tai.ted dimettb..i.oned dluwu:ng oJt. .1:i k.e.tc.h 1:iltow.i.119 -inteAttal. 6ea..tuJl.eA 06 dlf.tje/Lb, wood oft. c.oal. 6-Vt.ed boile/l..li, and
11.e.c.ovVt!f boil~.
I. Type of Fuel Burning Source TEWr:C:R FRAME #2 Stack Height Above Ground Level _Q ft.
Make and Model Number VicCREARY 21.J.O Volume of Furnace ft3
Inside Area of Stack 13. dt2
I Specify Ac tua 1 Amount of Each Fuel Used in A,bove Source ( s):
Coal lb/hr; Oil Grade __ Amount __ ·_ gal/hr, at __ BTU/gal and __ lb/gal or lb/hr
I Wood lb/hr; Natural Gas .6.ru)GJCF/hr, atJ..040 BTU/SCF; Other __________________ _
{Specify type, amount and heating value)
II Specify Maximum Rating for Each Fuel Burning Source:
SCF'/HH
(I Coal Oil Wood Natura.l Gas ..1.0.., OOOOther _________________ _
I Maximum Sulfur Content of Fuel
Type of Solid Fuel Burning Equipment Used:
Specify Standby Fuel __ Maximum% Sulfur
Hand Fired Spreader Stoker' _ Underfeed St.iker _ Chain Grate
Pulverizer_ Cyclone Furnace_ Other (Specify)
Traveling Grate
Ash Content of Fuel: Specify Method and Schedule of Tube Cleaning, if Applicable:
g Coal % Wood % Other Lancing _____ _ .Tube Blowing ______ Schedule ______ _
Emission Control Equipment (Describe in Detail in Sections IV and V)
g Collection Device: ~Ji:t __ Dry__ Steam Injection __ Air Injection
Draft on Boiler {Natural Induced ) cfm at __ oF
Total Number of Fuel Burning Sources Within Property Boundaries:
IS Collected Flyash Reinjected?
D Coal lb/hr Wood
Maximum Capacity Rating, by Type, for All Fuel Burning Units Excluding that Itemized Above:
lb/hr Oil __ gal/hr Natural Gas __ SCF/hr
(Total Like Units)
0 JV. SUPPLEMENTARY DATA FOR WET COLLECTION DEVICES
,j.A.tta..c/1 de.ta..il.c.d e11gi11ec-'Ung d,t.aw,lng.& 06 the. c.ontltol dev.i...ce a.1td )XV'...ti.cle .&lz.e vCJL,!,u..& tuvnova.l e.66,lU.c.nc.y c.Ultveb.
D Liquid Scrubbing Medium and Additives:
Total Liquid Injection Rate {Include Recirculated and Make-up Rates) __ gal/min or gal/1000 ft~
0 Operating Pressure Drop Across Device __ in H20
ANSWER FOLLOWING QUESTIONS FOR SPECIFIC DEVICE: B VENTURI SCURBBER: Inlet Area in2 Throat Area in2 Throat Veloci~y ft/sec
GRAVITY SPRAY CHAMBER: Number of Nozzles Liquid Droplet Size __ u Co-Current Countercurrent
D WET CYCLONE:
Body Diameter in Length in
PACKED TOI/ER OR PLATE TOWER:
Cross-Sectional Area _____ ft 2 Type of Plate ______ _
0 Inlet Area fo2 Number of Nozzles
Outlet .Area in2
Depth of Packing ____ _
Type of Packing _____ _
0 OTIIER WET COLLECTION DEVICES: GIVE COMPLETE DESCRIPTION
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Signature:·, __________________ _
I V. SUPPLEMENTARY DATA FOR DRY COLLECTION DEVICES I •A.t.tac.h de..:tJ:t.il.e.d eng-i..nee/Ung dtuzwi..ngf> 06 the cont/tot dev-<.ce a.nd ~c.le 6-i..zc. ve..wu..6 11.emoval e6i5-<.c£e11cy C!.LILVU.
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BAGHOUSES: Cloth Area ft2 ----Bag Material
Number of Compartments _______ _ Pressure -Dro·p Total _ _______ in H20
Method of Cleaning ________ _ Air-to-Cloth Ratio _________ ft/min
Time Between Cleaning mi ns ,. hrs
ELECTROSTATIC PRECIPITATORS:
GENERAL:
Effective Area of Grounded Collector Plates
Number of Compartments _or Chambers
ft2
Number of Cells per Compartment _____ _
ElecfriCal F·ield Gradient at the Discharge or Emitting Electrodes _____ KV/in
Average Electrical Field Gradient at the the Grounded Collecting Electrodes _____ KV/in
Fields of Treatment _____ Potential Applied to Emitting Wires ____ KV
SINGLE STAGE TYPE:
Distance Between Emitting ~/ires and Collecting Plates _____ in.
Number of Isolatable Bus Sections _____ Corona Power ____ Watts/1000 cfm
T\10 STAGE TYPE:
Distance Between First Stage Emitting Electrodes and Field Receiver Electrodes (Ground) ____ in
Potential Applied to Second Stage Emitting Plates KV
Distance.Between Second Stage Emitting Plates and Grounded Collection Plates _____ in
I CYCLONES/MULTICYCLONES:
Simple Cyclone Multicyclone
Diameter __________ _
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in Diameter , in
Inlet Dimensions of Individual Cyclone Inlet Dimensions ______ _
Outlet Dimensions Outlet Dimensions -------of Individual Cyclone
I in H20 Pressure Drop in H2D
Number of Cyclones
Pressure Drop ______ _
Number of Cyclones ______ _
.OTHER DRY COLLEC~ION OEVICES: GIVE COMPLETE DETAILED ENGINEERiriG DESCRIPTION ANO DRAWINGS •
• Signature: Title:
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--l!!!!!!!!!I !!!!!!!!
VI, AREA DIAGRAM
E!!!!I l!!!!l!I liiiiil liiil liiiil
· O.ner __ .[C:.!T?lTI.130..'.c'"c.Vi!:.1.K.JC.JQ.J.!,TJUu'.\Q.L:;J'3,2•)..:Ti:.J;;•wJ-"?i'-----
INSTRUCTIONS:
1. Show all surrounding buildings and roads within
1000 feet of subject equipment which is located
at center of circles.
2. Indicate location and type of building by the
use of small numbered circles with the de•
scrip.tion below.
J. Show roads as lines representing the road edges.
Indicate street names and highway nu~bers.
4. Show wooded or cleared areas by approximate
bounr' ry 1 i nes and the \lords 11woods". uc 1 eared 11
,
11cornfield11 • etc.
5. Indicate direction of north by arrow.·
EXAMPLE
DESCRIPTION
•Cristex Corpo~ation
Office
Boiler
G). Church
® Residence
X Indicates location of equipment. -· - --- - - -
e, ...
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DIVISION OF ENVIRO:iMK.'lTAL HA.'iAGEMENT
December 8,' 1978
!-1 E }I O R A :l D U M
TO:
FROM:
TllROUG!l'!
SUBJECT:
D:ivid Ligon
_Archdale Building
Ronald·Eawks, Regional Engineer
Air Qlla.lit7 H3nag6Clent·
Marahnll ltackley, Regional Sup~,rvisor
Ral,cigh Regional Office
SOC for Number 2 Tenter
Cristex Corporation
Attached 13 a Special Order by Consent ~bat:amcnt "of \ilsi'ble----.,=, .
...,.-.,..c,.,..... .... ~EY-ssiona .. from .. ~u.mb_e,,;:,._._t tenter frame at ~--i~t:e::;;: Cor?oration, Ox_for:l, . · ,.,.) ·
.. ----·-, Granville County. . --......._.) (' -···•-•·-.-. •••...... _,, ....• .,,=·· •·--·-··•··--·-·
~-~,~.--~-----.... ..--......... , _____ ,'<'~~.-o••·-~ ....... ___ ._..,,. • ....,, ... .-....... , .
.. The visible emi.5sion e~1:1luation included i-3 ne~1cral ~onths old,'
howaV.e:r t!lo v!.o;l..ation h:ln been ·determined to_bc the clir~~t result of
the volitilization of a mineral oil based napiJine a3ant. :.iserl on t:1e
nylon prior co !:leat s":t!.n;;. The plant has reduced the .fraqucncy of
processing this styl2 of cloth in recant months, but will continue
future processin:; ·as ::iar!,ct dem.:inda. Since it. is apparent that further
non-continuous violati,Jns will occur the conpany la proposing a abate-
ment plan. anr! the r:o;io::nl office concurs vith the schedule.
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NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT
AIR QUALITY SECTION
REQUEST FOR ACTION TO BET AKEN
/) \ . : ,( n I L.,Jr_._~-\µ
The item liste<l below requires action to ascertain compliance under Article 21, Chapter 143 of the t~~rnl Statutes of North Carolina, concerning rules and regulations governing the control of air pollu-
Cristex
Subject
I Revision of Permit
Im,•e2tigation Requested By
II Jim Patterson
lfamurka
Address
Oxford
Atlc.lress
CounLy
Granville
County
fl. CRAMR
~edTo
Date
11/27 /78
Plans Review
Investigated By
Bill Pearce
Date
2/21/79
Returned
Action Recommended
D Issue Permit No. 2097R2
ill,;ootlir.>tlon R<ll)Ort
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3.
4.
5.
6.
7.
Permit No. 2097R was originally issued for six atmospheric dye tubs, two No. 6
oil-fired boilers, tenter frame (No. 3) and a fiberglass mesh pad type mist
eliminator installed on tenter frame (No.· 1).
Cristex has applied for a permit to construct and operate a fiberglass mesh pad
type mist eliminator installed on tenter frame (No. 2).
The .mist eliminator is identical to that presently installed on tenter frame (No. 1)
(Ref: Application form) and tenter frame (No, 2) is the same type operation as
tenter frame (No. 1) (Ref: Jerry Clayton, AQ-16, 11/29/78). Therefore, compliance
with .0515 and .0521 can be expected.
Cristex is presently under S.O.C, for
a construction completion·stipulation
conditions of S.O.C.
visible emissions. The permit will contain
and an evaluation stipulation to reflect
NSR, NSPS, NESHAPS., and PSD do not apply--existing equipment,
The region recommends issuance of permit with stipulations for S.O,C.
This office concurs and will combine with existing permit No. 2097R, Issue Permit
No. 2097R2.
E Corroapondonce To:
I · Slgn11tun:
I Wh!t.e-Enl!lneorlne: Branch; Yollow-C.ntral File; 131uo-Regloriol Office
AQ-16 Rav. 7-1-71
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William R. Pearce
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DIVISION O'F l!.'iVIRONMENTAL 1'.A!iAGEME!iT
'February 23, 1979
·Mr. c • .J. O'l3ryant,-Executive Vice President
· Cristex Corporation.
"Industry Drive
Oxford, Horth Ca'rolins
Dear Mr. O'Bryant:
Subject: _Permit No. 2097R2
Cristex Corporation
Oxford, North Carolina
In accordance with your application received November 27, 1978, we are
forwarding herewith Permit Ho. 2097R2 to Criste7. Corporation, Oxford, !lorth
Carolina for the construction and/or operation of air pollution abatement
facilities and/or emission sources. ·
Thie Pernit shall ·be effective from the date of issuance until October
1, 1981, -is. nontransferable to future owners ,:md operators, and shall be
subject to the conditions and limitations as epec:!.fi_ed therein.
Fnclosure
cc: '!(.r. Stan· Taylor
Informntion Services
WRP/gae·
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Sincerely,·
Original Signed bll.
A. F. McROR,!l:l
A. F. Mc~rie, Director
Division of Environmental Hanogei:,ent
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NOil.TH CAROLIHA
EiNIROtlliE!ITAL l1ANAG!lHl!l1T COHMISSION
DEPARTiiE!iT OF !IATIJUL RESOURCES & COtlMUUITY D'EVELOPttENT
ltaleiRh
For the Dischar&e of Air Contaminants Into the Atmosphere
ln accordance vith the provisiona of Article 213 of Chapter 143, General Statutes
of Uorth Carolina aa amended, and other applicable Lava, Rulea and UeV,Ulations,
Plll\MISSIOM IS IIEREBY GRANTED TO
Cristex Corporation
Ittduatry Drive
Oxford, llorth Carolina
l'Oll. Tlll\
construction and operation of1
(1) ai:t atrat>apharic dye tubs (proceasin,. 1,600 pounds per hour nylon/
acet;.te cloth each)
(2) two tit,. 6 oil-fired lloilcra (25 :t 106 !lTU per !wur heat in;,ut each)
(J) a tenter f.ramo (lio. J)
and au air cleaning device conaist1ng of two fiberglass mesh pad type mist
eliminators (360 sqw,re feet of face arua each) anJ appurtonancos installed
on tentar !Tames (.lo. 1) and (!lo. 2) respectively to rc!IIOve particulate and
visible etdasiona, and for tho diachnrga of the treated air and associated
vaut and stack gaoes into tun outdoor atl!IOsphcro at its facility located at
Industry l)rive, Oxford, !forth Carolina, Granville County,
in accordauco with the application received Movt'l.lllbar 27, l97il, anu in confor-
mit7 with the plano, specifications, and other supporting data, all of which
are filed v:ith the Dupart.aent of Natural Roaourcee & Colll!llunity Developmont .und
are incorporatet! au p,n·t of this Ponaiit.
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Permit No. 2097R2
P11g11 2
1. Thia Permit aball becollO voidable unloaa tbll mist al:lminator on tenter framo
Ho. 2 ia coll.Btructed 1n accordance vith the approved plans, specifications,
and other supporting data on or before Juno 1, 1979 or es this date may be
amended.
2. The facilitieo elulll be properly opera.tad and mintained at all times in auch a
manner as to effect an ovarall reduction 1n air pollution 1n keeping vith the
application and otherwise to reduce air contamination to the extent necaaaary
to co1:1ply vith applicnble Environnomtal llanagRlll<mt Co-...nisaion llegul.at1ons,
includiuu 15 liCAC :m .051~, .0516, .0518, and .0521.
3. Reports on the operation and naintenanca of th~ facilities shall be submitted
to the Diviilion o! Enviroru.iant1tl }!Aua11<Am1ut et such intervals and in such form
and detail as WIY 'Ile required by the Diviaion. Information required 1n such
ruporta may include, but is not limited to. proceso vaigbt rates, firing rates,
hours of op11ratiou, and pravcntive mintenanco schedules.
4, Tbll mist eli:lliuator on tBUter lto. 2, ahall be QValuatod !or compli.'\nco with
Envtro~ntlll Managru:wmt Co.a;iisaion Re1,wlation(s) 15 llCJI.C 2D .0521 by the
Divieion of Cnviranaentcl lianage:annt, at the afore:,umcioned location, by
July l, 1979. This Permit oball beco:no voidlible, with proper notice to tl1e
company, if the results of the evnlW>tion indicate tlUlt tho mist olilldnator
does not Naet applicable laws, ruleu, and regulatione.
5. A violation of any terra or cou.litiun of this Pol"lllit shall subject the Pormittee
to onforcrn:,ent ;,rocedurcs contained 1n North Carolina General Statutes 143-215.114,
including 1.111oousi.ent of civil penalties.
Permit i11uued this the 2Jrd day of February, 1979.
llORTll CAit0LUlA Of'w"IR0!lllllii!AL MAliAGE?mllT COJ-ll:lISSl0li
Origin..J Signea ll11,
A. F. McROR!El
A. F. Y.cRorie, Director
Oivilli.au of I!nviroruauntal Manage,:ietit
uy Aut~ority of the Secretar;, of the Depart1:1Cnt
of llatural !tcsourcen & Co!ll.1unit;r Develop,,,ent
Pen.it !lo. 2097JU
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":·"'"
The Neu, & · Observer
215 South Hci.iowe 11 Street
Ra 1 e1 r:ih IIC
De4r Sirs:
OIVlSIOH OF EHVIROIL"IEIITAL MAlu'.GE.HEllT
EllVIRO!IJ-IEHTAL OPERATI0:-15 SECTll)/l
March 22, 1979
.. Referenca: Cr1stex Corporat1on
AQ-7&-2.13
. Attached hereto 1s one (1) copy of I liot1ca of ·Intent to Issue Spaci..il
Order and Opportun1ty for Pub11c C0ll'!l1Y.?llt on mat.tori; relating to th~ CQll1Pl1ancc
1t1tlJ Air Quel1ty Er.t1ss1oni Control Standards. It is requesti:d that you pub1isi'l
the attach<?d 1,ot1c:? 1ri 001,_ (1) -ccpy of your papc1· on or b<?fore ,\pr11 5, 1'17::1. . . .
· Pub11ca~1.:n char<;cs for the liot1ce w111 iXl paid.liy ·c.ih Office up,Jn riece1;it
of your invoice, tc'.)ethcr 1·11 til an aff1Jav1t of p1ib1fcatfan. Pl<!as.i: send twr.; (2)
cl'!p1..:s of tlu: aff1dnvi';: of ;,ubl1cat1oll alo:v; 11ith t:1ree (J) co,,i<:$ tlf. tr1e invoica
· to the unders 1 gncd. · ·
Enclosure
· · cc: Secretary Hotlard N. Lee
Mr. ·L. P.· Centon, Jr.
Mr. Stan Taylor
Mr. Paul Traina
Mr. Stuart Gaorge
· Mr. Jerry Cl J.yton
, Sincerely,
, Ii. Vance ilol t, Act1r.g Coordinator
Enforcer.wnt -l, E111ergency Response
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, I • l 1 STATE OF NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF NATURAL RESOURCES AND COMMUNITY DEVELOPMENT
RALEIGH, NORTH CAROL!Nft,
NOTICE OF INTENT TO ISSUE SPECIAL ORDER AND
OPPORTUNITY FOR PUBLIC COMMENT
NOTICE IS HEREBY GIVEN, by the North Carolina Environmental Management
Commission of its intent to issue Special Order by Consent AQ-79-213 to Cristex
Corporation, Industry Drive, Granville County, 1,hich is currently operating in
violation of air pollution control requirements contained in Title 15 of the
North Carolina Administrative Code. The proposed Order contains a schedule for
achieving compliance by June 30, 1979.
· Any person requesting a public hearing regarding this proposed Order should
submit a written request with a statement supporting the need for such a hearing
and a brief summary of the information intended to be offered at such hearing.
Any request for a public hearing should be submitted within 15 days of this Notice
to Mr. H. Vance Holt, Acting Coordinator, Enforcement & Emergency Response, Division
::.of'3Environmental Management, P. 0. Box 27687, Raleigh, North Carolina 27611. Any
person wishing to comment on this proposed Order m,,y do so by submitting comment to
Mr. Holt in writing within thirty (30) days of this Hotice.
Additional information on this Special Order is available for public review at
the Regional Office of the Department of Natural Resources & Community Development
indicated below.
Mr. Stan Taylor, Regional Supervisor
Division of Environmental Management
3800 Barrett Drive
P. 0. Box 27687
Raleigh NC 27611
Origln·•l Signed IJ,1
"-F. McROR!E
A. F. McRorie, Director
Division of lnvironmental Management
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NORTH CAROLINA
SPECIAL ORDER BY CONSENT
AQ-78-213
GRANVILLE COUNTY
IN THE HATTER OF UNAUTHORIZED
DISCHARGES OF AIR POLLUVl!TS
TO THE A.'IBIENT ATMOSPHERE BY
CRISTEX CORPORATION, OXFORD,
GRANVILLE CXlUNTY, NORTH
CAROLINA
THIS ORDER BY CONSENT made and entered into pursuant to North Carolina
Statute 143-215.110 and in accordance with the requirements of Section 113
of the Clean Air Act by Cristex Corporation, hereinafter referred to as the
CXlMPANY, with the North Carolina Environmental Management Commission, an
agency of the State of North Carolina, hereinafter known as the COMMISSION.
WITNESSETH:
I.
II.
The COMPANY does hereby stipulate as follows:
A. The CXlMPANY has operated and is now operating Tenter Frame No. 2 at
its facility located in Oxford, North Carolina.
B. Tne COMPANY has discharged and is now discharging to the ambient
atmosphere ~isible emissions in violation of Emission Control
Standard 15 NCAC 2D .0521 "Control Of Visible Emissfons."
C. The COMPANY has submitted an application for a permit to construct
and operate a fiberglass mesh pad type mist eliminator on Tenter
Frame No. 2 for control and compliance with 15 NCAC 2D .0521.
The COMPANY desiring to comply uith the legal requirements of the COMMISSION
regarding visible emission to the, ambient atmosphere and with all pertino·,1t
provisions of the law and applicable rules and regulations of the COMMISSION
does hereby agree to do and pe.rfo m all of the following things on or before
the dates hereinafter set out:
A.
B.
c.
D.
Let contract for visible emis8ior.s control syste□ on o~ before
January 2, 1979.
Begin construction a..'ld/or installatio!l of "";iisible. errissions control
equipment on or before April 2, 1979.
Complete construction and/ 0r ins tall a ti on of visible emissions control
equipment on or before June 1, 1979.
Achieve compliance with Emission Control Standard 15 NCAC 2D .0521
11 Control Of Visible Emissions," in the manner chosen and proposed by
the COMPAi.~Y in the above referenced permit application on or before
June 30, l~~:~\t..\:i14l7§p-3'~
~,:> {O
e:, MAY1979 ~ i:: rCENTRAL ~
~'? r/! E COD !)] ,i::.t .... ' , y ~-)
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SPECIAL ORDER BY CONSENT
AQ-78-213
Page 2
III. The COMPANY shall use gc;od engineering practice in operating and
maintaining Tenter Frame No. 2 so as to minimize visible emissions
into the ambient atmosphere during the period between the date this
Order is executed by the COHPA.'!Y _and the date specified in this Order
for achieving compliance with Emission Control Standard 15 NCAC
2D .0521 "Control Of Visible Emission."
IV. The COMPANY _shall submit no later than five days after the deadline
for completing each increment required in Section II, Certification
to the Director, Division of Environmental Management, whether such
increment has been performed.
V. In the event the COMPANY _fails to achieve final compliance with any
emission limitation, emission standard, or compliance schedule in this
Order or under the North Carolina Implementation Plan by July 1, 1979,
the COMPANY will be required to pay a mandatory noncompliance penalty
pursuant to Section 120 of the Clean Air Act, 42 U.S. C. Section 7420,
or North Carolina General Statute 143-215.114(a), if the Environmental
Protection Agency has delegated authority to collect and assess such a
penalty to the State of North Carolina. Nothing contained herein shall
prevent the United States Environmental Protection _Agency from taking
enforcement action pursuant to Section 113 of the Clean Air Act or the
COMMISSION from assessing a civil penalty pursuant to North Carolina
General Statute 143-215.114 for violating any term or condition of this
Order, including failure to achieve any compliance date which is scheduled
to be achieved in this Order prior to July 1, 1979.
VI. The COMPANY agrees that this Special Order shall pertain only to that
equipment or· source described in Section IA of this Order. Unless an
applicable Special OrdQr or Perr.ti. t lls.s beGn issued b:, the COMMISSION,
any violations of J\...ir quality .) Lnr: :!:1 rds, rc·sulti1;.g frc-m n the.r sourc:es
or equipment for -;\rhich the C!1l·il.'1\;TY !.; ~:r!:~pnns:iblf, shnll. :3ubject t!u::.
COJ:..iPP.l-rY to all sanctions prov:Ldc.d ;, ., ~~1.:r!.:h C.1-rolina CQneral Statute
143-215 .114.
VII. Failure cf the. COMPANY to cornrd.y \,ij .. th :my p rovisj_on i:on t:ainetl hereiu,
including Section III, or c.liscl1ar:,_;c:: fror;: Ten:.:cr Frame ~fr.·o 2 after
June 30, 1979 in excess of appJ.ic::blc st2,-:darcis, shall subject tl,e
COclPANY to all sanctions provided by North Carolina General St.1tute
143-215.114.
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SPECIAL ORDER BY CONSENT
AQ-78-213
Page 3
This the --~!A~1/~IZ~O'------day of ____ j~)'-'-l-'--IZ'--t_L_· _____ , 1978.
ATTESTED:
APPROVED AND ACCEPTED
W. Whitley, Ch irman
Environmental Marfagement Connnission
Date: -------------
CRISTEX CORPORATION
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.A. F. HcRorie, Secretary
Environmental Management
Commission
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CERTIFIED MAIL
RETURll Jl.ECBil'T 1tEQUESTltD
lir, C, J, .O'BryGDt
Executive Vice Proaident
Cristox Corporation
Induatry Drive
Ozford llC 27565
· i!iear Mr.' O'ilryant:
DIVISION OF ENVllONKBN'IAL KA?IAGEM!llff .
Hay 17, 1979
SUBJECT: Sped.al Order by CoWJent
AQ-78-213
Attachod you• will find the Spacial Order by Conoau.t vhich you have previoualy
signed. ThB ODClosed Order with ita compliance ochodule baa beGD aubje1ctcd to·
public cOl!llllOut, reviewed and approved by tho.North Carol:lna.Enfiroumontal Manage-
ment Commiaaiou at its May 10, 1979, meeting, The terms and conditioUG ea contained
therein are in full effect. ·
Add1tioaally, as required by.the Clean Air Act Amondmant of 1977, this Order
haa also boon eubmitted to the United Stateo Enviro=eutal Protection Agency for '
thoir approval of this doc·u:nont as a ''Delayed Col:l;>linnce Order". ·
Should thorn be any further quoaticnuJ or ways in vbicb this Divisioa .Cllll ha
of uaiat11X1Ce, pleaaa feel free to call on its ropresentativea· 111 youT area.
Attachment
cc: L. P. Benton, Jr. n. Vance Bolt
Kirt Cox·
Stan :raylor
JPC:mnf
Sincerely,
Oii3i;rnl Sig;;ed by
. r-7 i P. BENTON. JR. ; • P, Mc:Roria
/ DiTec~or
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MEMORANDUM TO:
THRU:
FROM:
SUBJECT:
DIVISION OF ENVIRONMENTAL MANAGEMENT
ENVIRONMENTAL OPERATIONS SECTION
Stan Taylor, Regional Supervisor
Raleigh Regional Office
H. Vance. Holt, Acting Coordinato·r~
Enforcement & Emergency Response
Jerry P. Clayto~ . .· .
Enf_orcement & Emergency Response
Special Order by Consent for:
Cristex Corporation AQ-78-213
May 18, 1979
The ·enclosed copies of the above Special Order are as they were signed by
the Environmental Management Commission at':their May 10, 1979, !lleet:l.ng. · All
dei:dlines on dates contained.in this SOC should be documented by inspection
and a copy of the inspection report is to be sent to Enforcement & Emergency
Response.
The final compliance date inspection should specify that provisions of the
SOC were met and that source is in compliance. If,. source has· not complied or
final compliance was not achieved then the regional recommendatiqn for enforce-
ment, ·if any, should· accompany the inspection report, along with any documentation
necessary·for showing the violation.
Enclosures
JPC:mnf
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NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT
AIR QUALITY SECTION
REQUEST FOR ACTION TO BET AKEN
The item listecl below requires action to ascertain compliance under Article 21, Chapter 143 of the
General Statutes of North Carolina, concerning rules and regulations governing the control of air pollu-
tion:
00025
Name ...------,-,:;--··-• ", ,..,..,,\.._. Cris tex ·
AJdres~
Oxford
Compliance Inspection -New Equipment Installed
Investigation Requested By
RRO
Remarks
Assigned To
RRO
Investigated By
B. T. Foust & Alan Gaines
Action Recommended
Address
Date
7-17-79
Await call for reevaluation of mist eliminator
Inveatiption Report
1. Mr. Bill Caulder was contacted at the plant.
2. The company had installed a new Brinks Mist Eliminator.
.--····-·· .. :· clJi.irily ··-.:...-...
Granville ·,,
County
Date
7-17-79
Returned
Z 18 79
3. The equipment was installed before the federal cut off of July 1, 1979.
4. The equipment could not be evaluated at this time. There was a malfunction
with the air blower and the filters were stopped up or something was wrong.
The unit will be put into proper working order and Mr. Caulder is to call
when the unit is back in operation.
BTF/dc
Col'Nllpondenco To:
Whfte-Enctneerlna: Branch; Yellow-Central File; l!fua-Regiorial Office
AQ-16 Rev. 7-1-71
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NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT
AIR QUALITY SECTION
RECEIVE,: OCT
REQUEST FOR ACTION TO BET AKEN
31979
The item listc<l below requires action to ascertain compliance under Article 21, Chapter 143 of the
General Statutes of North Carolina, concerning rules and regulations governing the control of air pollu-
tion:
00025
Compliance Inspection -Mist Elimator
Investigation Requested By
RR0
Remarks
Assigned To
RRO
Investigated By
B. T. Foust
Action Recommended
No further action
Inveatiption Report
Address
Date
8-9-79
County
Date
8-9
Returned
8-10-79
1. Mr. Bob Clewell, the plant manager, and Mr. Eill Coulter the plant engineer met with
the regional representatives Mr. R. H. Ferneyh.ough Chemist with Water Quality.
2. A tour of the facility was taken the mist eliminator was working and there was no
visible emission from the exhaust port, on the eliminator.
3. This plant is not a point source. Now that compliance has been met with the permit
no further action unless a complaint or some action by the company be imposed.
Correspondence To:
NSI 6-1-80 . Signature:
Whlte-Englneerlnr Branch; Yellow-Central Fila; 131ua-Raglonal Office
AQ-16 Rev. 7-1-71
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DISTRIBUTION
(Optional)
Yellow Copy
Blue Copy
White Copy
-Mon. Mgt./Central
-Regional Office
Permits
Enforcement
Stack Test
NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT
AIR QUALITY REPORT
REQUEST FOR ACTION TO BE TAKEN
Files
The item listed below requi_res· action to ascertain compliance under Article 21, Chapter 143 II of the General Statutes of North Carolina, concerning rules and regulations governing the
I) control of air pollution:
-00025 Point Source
1 Name
Subject
/----,Cristex Corporation
,--Add~ss
'-------.Oxford ·
County
Granville
I ~ngineering Evaluation -Semi Annual Inspection
Investigation Requested By Address County
I Remarks
RRO
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Assigned To Date
RRO
Investigated By Date Returned
Action Recommended
Investigation Report
1. Mr. Bill Coulter the plant engineer met with the regional representatives.
2. A tour of the facility was taken.
3, The plant operates 2 tenter frames-each one is controlled by mist eliminator.
The plant was operating only one tenter-frame and one mist eliminator.
This was a good opp:;rtunity for Mr. Coats to see the d.nside of a tenter frame
and also the inside of a mist eliminator and compare to a unit that was
operating.
4. This plant met compliance at the time of the visit.
5, Reschedule visit about 6 months from now.
Correspondence To:
bch Signature: I AQ-16 Revised November 29, 1979
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DISTRIBUTION
Yellow Copy -Mon. Mgt./Central Files
Blue Copy -Regional Office
(Optional) White Copy -Permits
Enforcement
Stack Test
NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT
AIR QUALITY REPORT
REQUEST FOR ACTION TO BE TAKEN
The item listed below requires· action to ascertain compliance under Article 21, Chapter 143 of the General Statutes of North Carolina, concerning rules and regulations governing the control of air pollution:
39-00025
~~ ~~"" l.r Cristex _;
'-subject
Address
Oxford
_ . .c✓-"Cotin'ty ·~ .. :----, ' Granville '
I Engineering Evaluation
Investigation Requested By
RRO
Remarks
I Assigned To
RRO
Investigated By
B. T. Foust n Action Recommended
Accept this as a compliance report u Investigation Report
Address
Date
12/19/80
1. Mr. Bill Coulter the plant engineer met with the regional representative. D 2. A tour of the tenter frames and mist eleminators for controls was taken.
County
Date
12/19/80
Returned
1/7 /81
3. Marometer for pressure drop on the mist eleminators were observed. No problems with
the tenter frames or mist eleminators were observed.
4. Action at this time is to file this report to bring the status of this plant on all requirements by this plant in to prespective.
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Signature: @:pt/: KM
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ltx. r-li.llia111 J. Coulter
Plant Engineer
Cristez Corporation
Industry Drive
Oz~ord, /iC 27565
Dear Mr. Coulter:
DIVISION OF ENVIRONNENTAL MANAGEMENT
Juno 23, 1981
SUDJECT: Application for Per:;,J.t
Cristex Corpo:!.'a.tlon
ox for,:., ~·-le
Granville Count:y
T!li:1 is to aci:nowledge r~cei;;t of your tipplica.tion on June 19, 1981 ·for
a "Per .. -:!l t to cc,nstruct aJ:id O,1:>Cr,ec.e Air Pollution ~!bu::~r.:€."1t Faciliti.:2s -and/or·
En-.ission Souz-ccs .,"
'.l'his ..:1.ppliCation ia being proces:;ed a.;~d revi0,.r1'~ b~,-·t!k"? ,.\alci.gl1 ~~eqiOnal Office, R.Jleiq11, Ncrth ·carolina. ·If. i,'DU haV(? nn~1 questions concerning t .. 11:; .mat::er, pl~•as.a feel free tc con t.Jci: .::!a .2 r:: t.'1e .~u::tl:-ur .::.:clo~".
LDG/DDJ/mp .
cc: Mike Sewell
Sincer&ly·,
Lars_ D. Gcdr-1in, P.::.~.
I 1er1:U t Superyi:;or
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NORTH CAROLINA
···-···ENVIRONMENTAL MANAGEMENT COMMISSION
RALEIGH
RALEIGH REG!Of~AL OFF/CE
APPLICATION FOR
A "PERMIT"
TO CONSTRUCT AND OPERATE AIR
POLLUTION ABATEMENT FACILITIES AND/OR EMISSION SOURCES
Filed By: _.....;:;.CRI=cSc.cTE=c.,Xc......c.C.c.ORP-,-O_RA:_T_I_ON ___ _
(Name)
INDUSTRY DRIVE
(Address)
OXFORD, NC 27565
AQ-22 Rev. 2/75
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NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
RALEIGH
APPLICATION FOR A "PERMIT"
TO CONSTRUCT AND OPERATE AIR POLLUTION ABATEMENT FACILITIES AND/OR EMISSION SOURCES
THREE COPIES TO BE SUBMITTED
Fourth Copy Should be Retained by Applicant
To: Environmental Management Commission
Post Office Box 27687
Raleigh, North Carolina 27611 Date: ,Tqoe 19, 1981
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Caro}ina as amended, application
in the County of Granville at Drive Oxford NC
Company if Applicabfef Street and ity or Town Address of Plant or Facility
for issuance of a "Pennit" to construct and operate air pollution abatement facilities and/or emissions sources at above
location as specified in the accompanying drawings, specifications, and other pertinent data:
1. Nature of Operation Conducted at the Above Facility:
Textile-Knitting-Dyeing and Finish
2. Description of Process(es) Whose Emission(s) is/are to be Controlled by the Facility or Source(s) Which is/are to be
ConstructE!d or Altered. (Complete Section I)
New Boiler--Cleaver-Brooks Water Tube, Model DL-60
3. Furnish Type and Narrative Description of Proposed Control Device(s). (Complete Appropriate Supplemental Data Sheets for
Control Device to be Installed and/or Operated. Include Make and Model Number of Control Device(s) and Number of
Identical Units).
4. Contaminant
Emitted:
Weight Rate of Emissions (lb/hr):
Without Control Device With Control Device
5. Name and Address of Engineering Firm that Prepared Plans:
Carolina Boiler Sales & Service
6. Ultimate Disposition of Collected Pollutants:
8.
None
Indicate Period of Time for Which Facilities
are Estimated to be Adequate: _l2_Years
Name: ~ \ \\' ca.w. ~ ' C111iu.\olw.-lllT, .... , .. {Responsible Individual of Company Purchasing/
Operating Facility ... PLEASE PRINT)
Signature and Title:
AQ-11 Rev. ll/73
Co,1trol Efficiency (%):
Without Control Device With ContrqL Device
TodJ1stry Drive
Oxford NC 27565
Telephone Number: 919-693-6141
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I. GENERAL DATA FDR PROCESSES
• Atta.ch de.,tiu,te.d p!I.OC.eA.6 ·ettgJ..tte.C'Ung dltawing.6, e.qu..i.pne.n-t dltaw.utg.6 a.nd. 6low CWI.911.am.6 601t the. p!I.OC.e.h.6 ( e.6 l Oil .60U/l.Ce. (.6 I
bUttg c.oiv...tw.c.ted on. a.Uetted.
Name of Process : _.eBo~ieale,ea,r~f..;.,o~r'--"Pro:..:s.i!G.ce=S,aS'-"S\lY.llSs_tuec,mllL ____ _
Total Weight of Materials Entering this Process: ____ lb/hr or ton/hr
Volume and Temperature of Air Flow Entering Control Device: CFM@ --~-°F
Volume and Temperature of Effluent at Discharge Point to Atm_o_s-ph_e_r_e_:_ CFM@ ____ °F
Pollutant(s) tc be Controlled:
Height of Process Stack or Vent Above Ground Level _____ ft. Inside area of Stack _____ ft2.
Particulate Emission Rate (Before Control) _______ lb/hr
Particle Size Distribution: D-5p ___ %, 5-lDp____j,, 1D-20p____j,, 20-30µ____.l,, 30-40p____j,, 4D-50p____j,,>50~____j, I Gaseous Emission(s): Name (Chemical Formula) Vg/m3, PPM or lb/hr
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II. SUPPLEMENTARY DATA FOR INCINERATORS (Including Conical Incinerators)
Circle Type of Waste or Indicate Composition: Type 0 Type I Type II Type Ill Type IV
Combustible: % Non-Combustible: ___ % Moisture: ___ % Heat Value: ___ BTU/lb
Total Waste Generated Per Day: ___ lb. Hours Incinerator will be Operated: ___ hrs/day
Design Capacity for Above Waste: ____ lbs/hr Manufacturer and Model Number; Approximate Cost:
Primary Chamber Volume: ft.3 Secondary Chamber Volume: ft.3
Air Requirements: Total Excess Air % Draft: Natural Induced Other
Overfire Air: cfm Underfire Air: cfm
Is there an Electronically Controlled, Exhaust Gas Temperatu'reModulated, Damper Installed on the
Conical Incinerator for: Ove~fire Air Supply __ , Underfire.Air Supply , Dome Temperature set Point
Flame Port Temperature: ___ °F Secondary Chamber Temperature:-==-°F --
'Is there a Continuous Exhaust Gas Temperature Recorder? Yes No
Stack: Inside Ar_ea __ ft.2 Height __ ft. Gas Velocity __ ft/sec Temperature OF
Is there a Wet ScruOber?
Yes · No Flow Rate of H20 into Scrubber __jlal/min
Aux. Fuel: Oil Gas Other Burner Rating: Primary Chamber
____ .BTU/hr
Fan Capacity __ cfm
Primary Burner: Is there a Preheat Timer? Yes No Preheating Time:
Secondary Burner or Afterburner: ls there a Timer? Yes No
Is the Timer P~set by Charging Door? Yes No
Stack lined?
Type of Feed: Manual Automatic If Automatic, Describe ____________________ _
Distance from Incinerator to Nearest Structure(.s) in which People Live and/or Work. ___ ft.
Signature: Title:
-2-
I III. SUPPLEMENTARY DATA FOR FUEL BURNING SOURCES
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"Attac.h dc.ta,Lf.c.d diincM-i.On"-d d,wlkng alt J/u1,tch J/icwi1t9 .i.,ttc-tnal. 6c.a..tuJtu 06 d-'tf/CJL..!>, wood o,'L c.oa1. 6-<.,te.d ba.i.1.c,'L!l, a;u:i
'le.c.ovc.'ty boilc:w.
Type of Fuel Burning Source ~Bo=--"--'-il=--erc.:.. _____ _ Stack Height Above Ground Level 36 ft. Inside Area of Stack _220 ft2 I Make and Model Numbe.Cleaver-Brooks DL-60 Volume 'lf Furnace 1050 ft3
Specify Actual Amount of Each Fuel Used in Above Source (s):
lb/hr; Oil Grade _6_ Amount 414 gal/hr, at __ BTU/gal and __ lb/gal or lb/hr I Coal
Wood lb/hr; Natura 1 Gas 61M SCF /hr, at BTU/SCF; Other ___________________ _
I {Specify type, amount and heating value)
Specify Maximum Rating for Each Fuel ~urning Source:
I Coal Oil _/JJi_ Wood Natural Gas ..J(_ Other-----------------~--
Maximum Sulfur Content of Fuel 2.1 % Specify Standby Fuel Maximum X Sulfur 2.1 I Type of Solid Fuel Burning Equipment Used: Hand Fired
Traveling Grate
Spreader Stoker
Pulverizer
Underfeed Sf-."lker Chain Grate
Cyclone Furnace Other (Specify) ______ _ I Ash Content of Fuel: Specify Method and Schedule of Tube Cleaning, if Applicable:
Coal % Wood % Other Lancing ______ _ Tube Blmling _______ Schedule ______ _ I Emission Control Equipment (Describe in Detail in Sections IV and V)
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Collection Device: Wet Dry Steam Injection
Draft on Boiler {Natural Induced cfm at
Total Number of Fuel Burning Sources Witt1in Property Boundaries:
Air Injection
__ of
Is Collected Flyash Reinjected?
Maximum Capacity Rating, by Type, for All Fuel Burning Units Excluding that Itemized Above: (Total Like Units) I Coal lb/hr Wood 1 b/hr Oi1 __ gal /hr Natura 1 Gas __ SCF /hr
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IV. SUPPLEMENTARY DATA FOR WET COLLECTION DEVICES
*Atta.ch d(~frtLf.i!.d c.1tg-<.1:t:e-'Li.n9 d:uul1i.f!::J6 05 the. c.cmt/wt dc.,.1ic.e. a.nd pa,'Lt{c..ti!. Jize VC.'L6M .'L('Jl10v,u:'. eS6ic.iency C.U.·'tVLl.
Liquid Scrubbing Medium and Additives:
Total Liquid Injection Rate (Include Recirculated and Make-up Rates) __ gal/min or gal/1000
Operating Pressure Drop Across Device __ in H20
ANSWER FOLLOWING QUESTIONS FOR SPECIFIC DEVICE:
VENTURI SCURBBER: Inlet Area in2 Throat Area in2 Throat Velocity ft/sec
GRAVITY SPRAY CHAMBER: Number of Nozzles Liquid Droplet Size u Co-Current
WET CYCLONE: PACKED TOWER OR PLATE TOWER:
Body Diameter in Length _____ in Cross-Sectional Area ft2 -----
Inlet Area in2 Number of Nozzles Length ___________ ft
Outlet Area in2 Number of Plates
Type of Plate _______ _
Depth of Packing
Type of Packing
______ f,t
OTHER WET COLLECTION DEVICES: GIVE COMPLETE DESCRIPTION INCLUDING DESIGN PARAMETERS AND DETAILED ENGINEERING DRAWINGS.
Signature: Title:
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V. SUPPLEMENTARY DATA FOR ORY COLLECTION DEVICES
*Attach dc.t.tu.'led cngi11e.e1U.ng cl'UlWi.ngJ 06 the. c.on.Owf. de.vice and pa,'LU.d.e ~i..::e. l.'C'1..5M 11.emova£ e.C6(e,(e.11ct1 c.u.,'tve..~.
BAGHOUSES: Cloth Area ____ ft2 Bag Material
Number of Compartments ______ _ Pressure -Drop Total ________ in HzO
Method of Cleaning ________ _ Air-to-Cloth Ratio _________ ft/min
Time Between Cleaning mins, hrs
ELECTROSTATIC PRECIPITATORS:.
GENERAL:
Effective Area of Grounded Collector Plates ft2
Number of Compartments or Chambers ____ · Number of Cells per Compartment _____ _
Electrical Field Gradient at the Discharge or Emitting Electrodes _____ KV/in
Average Electrical Field Gradient at the the Grounded Collecting Electrodes ____ KV/in
Fields of Treatment _____ Potential Applied to Emitting Wires ___ KV
SINGLE STAGE TYPE:
Distance Between Emitting Wires and Collecting Plates _____ in.
Number of Isolatable Bus Sections _____ Corona Power ____ Watts/1OOO cfm
TWO STAGE TYPE:
Distance Between First Stage Emitting Electrodes and Field Receiver Electrodes (Ground) ____ in
Potential Applied to Second Stage Emitting Plates ____ KV
Distance Between Second Stage Emitting Plates and Grounded Collection Plates ____ in
CYCLONES/MULTICYCLONES:
Simple Cyclone
Diameter ---------
Inlet Dimensions ______ _
Outlet Dimensions ______ _
Pressure Drop
Number of Cyclones ______ _
in
Multicyclone
Diameter _________ in
Inlet Dimensions of Individual Cyclone _____ _
Outlet Dimensions of Individual Cyclone ____ _
Pressure Drop ________ in H2O
Number of Cyclones _____ _
OTHER ORY COLLECTION DEVICES: GIVE COMPLETE DETAILED ENGINEERING DESCRIPTION ANO DRAWINGS.~;,';:--_
/:; i.. . ·_':.' •. ,·,·::\
Signature: r::· . JUL Joe . \ Title: ,. -.(Tf -···'
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VI. AREA DIAGRAM
----------
~00 0 ,,/'. /
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---E~ ,/
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Owner cti5;.'.TEJt co.,.'l'
Location l\'\~u•\,nt£"" , OJtPortD fll,t {Give Stree ddressf -'
INSTRUCTIONS:
1. Show all surrounding buildings and roads within
1000 feet of subject equipment which is located
at center of circles.
2. Indicate location and type of building by the
use of small numbered circles with the de·
scription below.
3. Show roads as lines representing the road edges.
Indicate street names and highway numbers.
4. Show wooded or cleared areas by approximate
boundary lines and the words "woods" 1 "cleared0
,
11cornfield11 , etc.
5.
CODE
G)
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Indicate direction of north by arrow.
DESCRIPTION
Cristex Corporation
Office
Boiler Room
EXAMPLE G) Church
® Residence
X Indicates location of equipment,
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DISTRIBUTION
Yellow Copy -Mon. Mgt./Central Files
Blue Copy -Regional Office
(Optional) White Copy -Permits
Enforcement
Stack Test
CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT
AIR QUALITY REPORT
REQUEST FOR ACTION TO BE TAKEN
The item listed below requires action to ascertain compliance under Article 21, Chapter 143 II of the General Statutes of North Carolina, concerning rules and regulations governing the II control of air pollution:
39-00025 M Name
Subject
Cristex
Address
Oxford
County
Granville
D SIP Major Source
Investigation Requested By
Inspection -Permit follow-up-Engineering Evaluation
Address County
m Remarks
RRO
Iii Assigned To Date II RRO
Investigated By Date
I) B.T. Foust, Lars II Action Recommended
Godwin, William Dail 6-22-81
Returned
6-23-81-
Await letter of reguest for Permit Stipulation #6 oil Limitation Iii Investigation Report
IJ 1. Mr. Bill Coulter, the plant engineer, met with the regional representatives ..
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The plant is seeking a bond referendum for water recovery.
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The plant has installed a new natural gas/oil fired boiler, with 62,000,000
BTUs. The attached sheet has calculations that assume the plant will ~·d,5~t·
for a permit stipulation limiting the plant to operate the new boiler on #6
oil no more than 236,580 gallons per year. Mr. Coulter is to send a request
for the stipulation.
The present permit No. 2097R2 expires October 1, 1981 and is for the construc-
tion and operation of:
1. six atmospheric dye tubs (processing 1,800 pounds per hour nylon/acetate
cloth each)
2. two No. 6 oil-fired boilers (25 x 106 BTU per hour heat i2put each)
3. a tenter frame (No. 3)
and an air cleaning device consisting of two fiberglass mesh pad type mist
eliminators (360 square feet of face area eac,1) and appurtenances installed
on tenter frames (No. 1) and (No. 2) respectively to remove particulate and
visible emissions, and for the discharge of the treated air and associated D. Corr.espondence To:
[ AQ-16 Revised November 29, 1979
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· ID3 4al \ ,... )
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(Optional)
Yellow Copy
Blue Copy
White Copy
-Mon. Mgt./Central
-Regional Office
Pennits
Enforcement
Stack Test
NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT
AIR QUALITY REPORT
REQUEST FOR ACTION TO BE TAKEN
Files
I The item listed below requires action to ascertain compliance under Article
of the General Statutes of North Carolina, concerning rules and regulations I control of air pollution:
39-00025
21, Chapter 143
governing the
Address
Oxford
/_CountY-'---
Granville ·------
I Investigation Requested By
Wi 11 i am J, Cou] ter
Address
Oxford
County
Granville
Remarks
Date
6 25 81
:·' j •. -,.. .. . _,. __ .-,_ -: '.:.:~.r
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Date
6/19/81
Returned I Action Recommended
Issue Permit No. 2097R3 0 Investigation Report
1. Apglication is made for the operation of
10 BTU per hour maximun heat input) for
in operation May 11, 1981).
a new natural gas/No. 6 oil fired boiler (61 x
the purpose of process steam (boiler was placed D
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A letter was received 6/23/81 from Cristex requesting that the total usage of No. 6 oil
for the entire facility be liQited to 236,580 gallons per year (Ref. letter dated 6/23/81)
There are two existing boilers at the facility which burn natural gas with Ho. 6 oil as a
standby fuel. However, Permit No. 2097R2 shows these boilers to be burning only No. 6 oil
This must have been an oversight when the permit was issued because the application (re-
ceived January 11, 1978) indicated that both natural gas and No. 6 oil would be burned in
these boilers (25 x 106 BTU per hour hear input each). The permit will be changed to re-
flect the proper fuels.
Estimated potential or actual particulate emission rate: lO(s) + 3 = 10(2.1) + 3 = 24 lbs
1000 gallons, (24 lbs/1000 gallons)/(148 x 106 BTU/1000 gallons) = .16 lbs/106 BTU (Ref.
AP-42, Table 1.3-1). Allowable emission rate: E=l.09 q-0.2594 = 1.09 (111) -0.2594 = .32
lbs/106 BTU where Q = (2)(25 x 106 BTU)+ (61 x 106 BTU) =. 111 x 106 BTU per hour total
heat input. Therefore compliance with 15 NCAC 2D .0503 can be expected.
m Correspondence To:
Signature: I AQ-16 Revised November 29, 1979
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llr. WJ.lJ.1am J. coul ter
.Plant BngJ.neer
Cr1stez CorporatJ.on
Indlllltr!/ DrJ.ve
DIVISIOIJ OF ENVIRONNISN'l'AL IUINAt:BIIBY'l'
June 26, l98l
O11ford, North Carol.1.aa 27565
Dear llr, Coulter:
SIJTJJBC'J:1 Perm.it No.· 2097RJ
CrJ.stex Corpora.ti.on
Oxford, NC
GranvJ.lle County
. In 11ccordanca vi.th 11our applJ.c:4tJ.on recol.vad June l9, l98l, we are for-·
ward.tne herewJ.th Pormi.t No. 2097R3 to Cri.stex Corporation, OJCford, North
Carolina for the constructJ.on and/or operatJ.on of aJ.r pollution abatement
facJ.lJ.ties and/or eml.asion soorces.
If itn9_ parts, requJ.r-rits, or · lJ.mi ta ti.ans containad .1n t11J.s Pertili t
are una=eptablo to l/OU, !/OU haw the rJ.ght to an adjud.1catory luulring oofore
. a bearJ.ng offJ.cor &1.POJl written -demand to tho Director wJ.t!JJ.n 30 dags ·foll0'11-
J.ng rectJJ.pt of thJ.s Permi.t, J.dentJ.i'ying the speci.fic '1.ssuos to be contended.
Unless BUClJ delDBJld ls llllldO, 'this Permi.t shall be final and bin4J.nq·. ' .
T,'l.1s · F~rm.i.t at.all be effecti.ve from the date of issuance until AprJ.l l,
l9ft6, J.s noatransfer.tbla to future owners and operators·, and shall be subject
to the condJ.ti.ollB and lJ.mJ.tatJ.OD!i 1111 specJ.fJ.ad therein.
Sincerel !I,
KS/DDJ/mp
Enclosure
=• R • .Stan '1'4!/lor
Regi.OMl OffJ.co ltanJJ.ger
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NOll'rH CAROLINA
BNVIRONKBN'I'AL HANAGBNENT COHHISSION
DEPARTMENT OF IIATURAL RESOURCES & COKNUNI'rY DBVBUJPNENT
-Ral,dgh
, For the Discharge of A1r Contaminants Into the Atmosphere
------------------,--,--'----,--,----,---c-----.-----e-:-,-----,,------:,-In accordance with the provisions of Article 2lB of Chapter 143,·General Statutes of I N~rth Carolina as B11Jended, and other applicable Laws, Rules and Regulations,
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PERHISSION IS HBREBY GRANTED 1'0
Cristez Corporation
Oxford, North Carolina
FOR THE.
construction and operation of:
l •. One natural gas/No. 6 oil fired boiler (61 wi.llion BTU per hour mazimum heat in-
put) and
I operation of, ·
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2.
3.
2w natural gas/No. 6 oil fired boilers (25 m1ll1on BTU per hoar mazimWll-heat
input _each}
Siz_atmoapheric dye
each}
tubs (processing l,800 pounds per hour nylon/acetate cloth
A tenter frame (No. 3)
and a.tr clean.fng devices consisting of two mesh pad typo mi.st el.tm.tnators (360 square
feet of face area each} and appurtenances installed on tenter frames (llo. l) and (No. 2) I respectively to remove particulate and visible em1ssions, and for t.~e discharge of the
treated. air and associated stack and vent gases into the outdoor atmosphere at its fac1-
lity· located at Industry Drive, Ozford, North Carolina, Granville County, ·
I .!n accordance with the application received June 19, l9Bl~ and in conformitg with the -
plans, Slpecification and other supporting data, all of which -are filed with the Depart-
Ill ment of Natural ReS1ources & Community Development and are incorporated as part of thi_s·-_-11 Permit. _ _
· This Permit shall be e.ffective frOJJJ the data o.f its issuancs until Aprill, 1986, --:· I is nontransferable to future owners and operators and shall be subject to the following ..
specified conditions and limitat:J.onsT _ · -·.
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The facilities shall be properly operatsa aad. =intail!ed at all times in Sl_u~··a· -,_, · _,,:;;:
IIWUU]er as to effect an overall reduct:J.on in air pollution in keeping with-,t.he appli-_•· i;:.-·
cation and otherwise to reduce air contamination to the eztent necessarg to'·C0111p1,j9''
with applicable Environmental Management Commission Regulations, including 15 NCAC
2D .0503, .0515, .0516, .0518 and .0521 and in no case shall-the sulfur dioxide ·
· emi.saiollB from the boilers ezceed 2. 3 pounds per m.illion BTU input.
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.• Perm1t No. 20971U
Page ho
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2.
6.
Reports on the operatJ.on and maJ.ntenance of the facJ.lJ.tJ.es shall be subm1tted to the
DJ.vJ.sJ.on of Env1ronmental Hanagement at such 1nte:r:vals and 1n such form and deta.1l
as mg be roqa1red bg the DJ.v.1s1on. Informati.on requ.1:r:ed J.n such reports mag 1nclude,
but 111 not l.1m1ted Co, p:r:ocass ttei.ght rates, t.1r.1ng rates, hours of opsratJ.on and
p:r:event1ve .maJntenance schedules. ·
When parc.tculatdl and/or v1sible emi.ss.1ons due Co a malfuncc.ton of the process or con-
. trol equ1pment are or may be 1n ercess of Bnv1:r:onmental Management Comm1ss1on Regu-
latJ.ons, the Rc,g.1onal supervisor, Ral,91.gh Reg.1on (9l9) 733-2Jl4, of Cha DJ.vision of
Bnv:lr~ntal Nanagement shall be not.1fiecI as p:r:omptl9 as possible, but 1n no case
latar th.an twelve (l2) hours follO'o1.1ng the start of such mlfunctJ.on. Such not.1ce
shall spec.1f9 the nature and cause of the malfunctJ.on, the t.tz:,e r.-hen such 11'.alfunct.ton
r.-as f.trst observed, the ezpected duration and an estJ.mte of the rate ot emJ.ssJ.on.
2'he term lll4lfunctJ.on shall not be construed to .include start-up or shut-down pe:r:.tods
when pa:r:t.1culats, v.1s1ble or odorous amiss.tons erceed Env1:r:onmsntal Jtanagement Com-
m1ss.1on Regulac.tons when the durat.ton of such per.tad .ts less than ono hour. Further:.
II/Dre, an9 per1od of durat.ton one hour or. greater wlien partJ.culate, v.tsible or odorous
emJ.ss.tons e;rceed Bnv.t:r:onmental Management Commi.ssion Regulat1ons shall be construed
as a malfunct.ton.
-.:
All boilers shall ba restr1cted to a total combined usage of 236,580 gallons of No. 6 oil
per gear.
CrJ.stor CorporatJ.on, at least n.tnatg (90) dags pr.tor.to the erp1ration of this Permit,
shllll request .!ts extension bg letter. The letter should include the perml.e· number
_and a descr1pt1on of l!IOdi.fications, if any, that have been made.
This permit .ts subjoct· to revocat.ton or modificat.ton upon a determinatJ.on that infor-
matJ.on conta.ined in the appl.tcation or presented in support thereof .ts incorrect;
cond.tt.tons under which ·the permit renewal was granted have c.'1.anged, or violat.tons 0£
condit;J.ons conta.tned in the permit have occurred.
A violation of anl} term or condition of this Perml.t shall subject the Permittee to
enforcement procedures conta.tned in North Carolina General statutes l43-2l5.ll4,
including assessment of civil penalt1es.
Permit .tssued this the 26th day of Juno, l98l.
lio. 2097RJ
NOR'I'H CAROLINA BNVIRONMBN'rllL MA!IAGEHEll'I' · COMMISSIO!I
Kenneth Sc:huster, ActJ.ng Reg.tonal supervisor
D.1vision of Environmantal Manage111Dnt ·
BIi Authority of the Env.t:r:onmental Managemsnt
ComaJ.ss.ton