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Home My WebLink AboutNC0001606250_19990630_Cristex Drum_FRBCERCLA PA SI_Integrated PA SI Volume II - Appendix B and References 4 - 12-OCR., I I ,I· I 1•= ·I I I '. I I I ·I I I I I I I I STATE OF NORTH CAROLINA Department of Environment and Natural Resources Division of Waste Management Supe,fund Section INTEGRATED PRELIMINARY ASSESSMENT/SITE INSPECTION (PAIS/ VOLUME II APPENDIX BAND REFERENCES 4 THRU 12 Cristex Drum Site NCO 001 606 250 Oxford, Granville County, NC Reference No. 06597 June 1999 Jeanette Stanley Eni>ironmental Chemist Division of Waste Management Supe,fund Section I I ' ' NC Dtpanmcnt of Environment, Health, &. Nawnl ~~ourccs Solid Wane Marugcmcnt Division SAMPLE ANALYSIS REQUEST St.ate Laboratory of Public Health . P.O. Box 25047, 306 N. Wilmington St. R.aleii;h, Nonh Carolina 27611-8047 lite Number. · N;,_,neofSiu: /JC O (20 I (oo(p 2.<1J Samp!elDNuml C0·019-GU 08/13/98 1020 GRAB . . U12345678 C0081098, NC D. WILSON. li1eloc:i1ion C · d ·· :: ,:; ·fe . eoll tea B . PGRA01rnr FRoH LAGooN Cl<'. X ~n.1 m '-1 '--' ec y --!NORG-CLP . HETALS Ground Water fJ 'I. -/:a. r J tJ C,,, Dau: Collected ) I lgency: Hazardous W asu: Solid W asu: _0uperfund TCLP Compounds ---- 122 - Sample Type Inorganic Compounds Results(mg/1) I Environmental Concentrate Comments arsenic -barium - Ground Waler (1) Solid (5) cadmium --- L -chromium Surface Water (2) Liquid (6) -lead --mercury .-Soil (3) Sludge (7) selenium -silver - --Other (4) -Other (8) - -l -Organic Chemistry Inorganic Chemistry - l~arameter · Results (mg/I) ~eter· Results(mg/1'.(p ll·a,l. Organic Compounds Results(mg/1) , _ P&T:GC/MS antimony ,__ e:i ◄ c;,06:> -benzece -Acid:B/N Ext. ~senic L...o:OI carbon tetrachloride - t: 2,4-D , b,lrri.um ,. L... £) -I ------·· chl o rd.ari e -----------· --.--··------··--- 2,4,5-TP(Silvex) _ beryllium -chJorobenzene ~ chlordane . ~ mi urn L.o.s,o5 chloroform -beptachlor -chloride -o-cresol hexachlorobenz.ene ~omiurn L.c,. QI -m-cresol bexachlorobutadiene cobalt p-cresol ~pper -endri.n <:.c -o 5 cresol I 1: -lindane fluoride 1, 4-dichlorobenz.ene -- methoxychlor iron 1,2-dichloroethane --- I tox.aphene ~ad "'-0-Q05 I, 1-dichloroethylene -- --manganese -2, 4-dichlo roetby lene -~ercury L.,o «.:,DO 5 heptachlor - -~eke! c.,;;i'l -hexachlorobenzCne -nitrate bexach19robutadiene ~enium - .<'..o .G 3 ~ hexachloroetliaae -~ver <'...Q • a c, -methyl ethyl ketone FOR LAB USE ONLY -sulfates nitrobenzene .Date Received -thallium pentachlorop_benol -- -vanadium pyridine -..k:::""zinc <'...D=o5 -tetraChloroethylene .Date Extracted -pH trichloroethylene --conductivity 2,415-trichlorophenol -Date Analyzed TDS 2, 4, 6-1rich1orophenol -- IReporle<l By -flash point -vinyl chloride ' ---endrin lindane -- Date Re{}orte<l methoxychlor I 1.1.130 AUG li98 -- --toxaphene ub Number 2,4-D -- --2,4,5-TP (Silvex) IDHS 3191 (R~vi5cd 12/93) I . ' SAIVIPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Sl. ll. • NC I)~~~mcnt of Enviionmcnt, IJ Health, & N.aOJ['I.I RCJiiources Solid Wut.c Man.agcment Divi,ion R.alei1:h, North Carolin.a 27611-8047 llteN_ u_mbc_ r lit Q (20 / (oo(p :2.<V Sample!DNuml ,.co-002-GW 08111/98 1250 GRAB RECEIVED II ...J..!!.~-"'-<Ll<'--.L""'-':.J.<....lA..cL-""'----12345678 C0081098, NC D. WILSON O~_T D91998 jamcofSite 'teLoc.:i.tio Do✓ t'.Y1 5, -fe--, Collected By_·· IHORG·CLP METALS Ground Water /J y_ -bJ_ r/',~ /1.} G Date Collected · SUPf?ffeUNO SECTION Cridex n --I ·-- lgency: HawrdoU5 W a.ste Solid Waste _0 u perfun d TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) I Environment.a! Concentrate Comments -arse.:::uc barium - Ground Water (I) Solid (5) -cadmium ---I_ chromium - Surface Water (2) Liquid (6) le:id -- -mercury .-Soil (3) Sludge (7) selenium --silver - -Other (4) -Other (8) - I - -- Organic Chemistry Inorganic Chemistry - tarameter RLSults (mg/I) P/4eter Result.s(mg/1,lili, 'C. Organic Compounds Results(:ng/1) P&T:GC/MS _,_ antimony ,(_ D, D,eZ'2. benzene - Acid: BIN E~L .....j,...,-"1S eni C .;:_ 0 ,.c:, I c:irbon tetrachloride '== 2,4-D. - --b.~J,-'<tium . ____ Q,__j ---chlordane -·--·-·-·····-· ·····-···-· 2,4,5-TP(Siivex) _ beryllium chlorobenz.ene . - - chlordane --~d mi u rn ~0.005 chloroform -. -I= beptachlor -chloride -o-cresol hexac~orober:ze:it • --i---elrro mi urn <'._o-al -m-cresol hcxadilorobutadicni:: cobalt p-cresol fapper - I endrin -<-o.a.5 cresol - lind~,e fluoride I, 4-dichlorobenzene -- methoxych.Jor iron 1,2-dichloroethane --- toxa:;hene ~:id z~ . .:;i.::il;:'., -1, 1-dichloroethylene "· -nunganese -2, 4-dichloroetby lene ~ercury "--Cl QQO 5_ \ -beptachlor y-iiickcl 0 •lQ -hexachlorobenzene 11-Ilitrate . hexachlorobutadiene ~eniurn - .(__ 0 -D Q !5 ~ hexachloroethane - ~Iver L._c .o':'i -methyl ethyl ketone I FOR LAB USE ONL y -sulfates n.itrobenzene - -thallium pent.achloropben0l - Date Received vanadium pyridine - -~zinc L_~ -Q .5. -tetra~hloroethy lene I Date Extracted -pH -trichloroethyleue -conductivity -2, 4,5-trichlorophenol Date Analyzed -TDS 2, 4, 6-t rich! orophenol -:I Reported By -t:ia.sh p(?int -vinyl chloride --endrin lindane -- 1 Date Reported --methoxychlor 01.t1i9 ~UG 1798 ·--toxaphene . Lab Numoer 2,4-D -- ---2,4,5-TP (Silvex) D_HS 3 I 91 (Revised l~/93) I 1 •. ' NC Dep~nmcnt of Environment,. / 1 Hullh, & N,om,J Ruou,m Solid Wutc Marugcmcnl Divi,ion SA..MPLE Ai'IALYSIS REQUEST St.ate Labon.tory of Public Health P.O. Box 28047, 306 N. Wiiminl"f"n St. 0.1.: .. , •• n lite Number NameofSili: liteLoQtion J f .----:: 2/98 1000 GRAB ,vto (!}0 / (oOUJ J.', ,0 Sample!Dl co-oo.-G~ .0088'1~98 --NC D. ~!LSON Cr,dex tJx-bJ.r,J 12345678 CD ' f)n,1 m ,,; , ·fe.---u:illectedB "E.lALS _ Ground ~ater . lNORG-CLP n Date Collecti I 29 Time ) 0uperfund TCLP Compounds lgency: Ha=dous W a.ste Solid Wa.ste ---- Sample Type Inorganic Compounds Results(mg/1) I Environmental Concentrate Comments arseruc -barium - Ground Water (I) Solid (5) cadmium --- I--chromium Surface Water (2) Liquid (6) -lead - -mercury Soil (3) Sludge (7) -selenium .--silver - -Other (4) -Other (8) - -r - Organic Chemistry Inorganic Chemistry - r::ameter Results (mg/I) ~eter Results(mg/1). '1 C Organic Compounds Results(mg/1) P&T:GC/MS antimony Zo-oo'-a benzene - -Acid: BIN Ext. ~senic ~. Ol carbon tetrachloride -I= 2,4-D -·-:-L--.,..P«ti I., ::1 0 ~ chlordane -------------·-· -·--·-·-·-·---· -·--··-----··----- 2,4,5-TP(Silvex) · _ beryllium -chlorobenzene chlordane ..j../"admi urn ..;,o. oo!S chloroform -- heptacblor . chloride o-cresol I= -- hexachloroben..zene ~a mi urn L.O.QI -m-cresol hexachlorobutadiene ~alt p-cresol -- endrin pper L....Q .q5 cresol -I lindane fluoride l ,4-dicblorobenzene --melhoxychlor iron l ,2-<lichloroethane -- -toxaphene ~ad ~-oc5 -l, 1-dichloroethylene I: -manganese -2, 4-dichloroetbylene ~ercury ~~.,gl)c,5 -beptachlor -~eke! 0. -04:i hexachlorobenzene -l-nitrate• bexachlorobutadiene ~enium - -<'..,Q,CQ5 ~ hexachloroethane - ~ver L-.o -o 5 -methyl ethyl ketone FOR LAB USE ONLY sulfates nitrobenzene --loate Received thallium pentachlorophenol --vanadium pyridine -_1:::::-_......zinc ..<..c.o5 -te:trachloroeth y lene .Date Ex1racted -pH -trichloroethylene -conductivity 2,4,5-tricblorophenol -Date Analyzed -TDS 2,4,6-Jrichlorophenol -I Reporied By -flash point vinyl chloride - --endrin lindane -- Date Reported -methoxycblor I 01.ii'.20 AUG 1798 - --toxaphene Lab Number 2,4-D -- --2,4,5-TP (Silvex) I OHS 319! (R~vi5cd l'.::/93) I , NC Dcp:!!tment oi Environment, Health,&. Nac.iral Resources Solid Wut.e Ma.n.agement Divi,1on SMIPLE A.i'{ALYSIS REQUEST St.Ate Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Raleii;h. Nonh C•rolina 27611-3047 l i·te· ·.Num .. be. r ..JM~t..""'-'OL.1.t2c.10.L.Ll ...... (o""o"'-"(p'-U2w-..J.<_V=---Sample ID Numb, C0-013-GU .. , 08/12/98 1715 GRAB 12345678 · CD081098, NC D; WILSON NameofSite Cr:i dex Dev m s, ·fe-ColleciedBy_··_. liteLoc:ition {)_ x -bJ. r,;j tJ C,, Date Collected !NORG-CLP METALS Ground Water 42 --I -· fgency: Hazardous Waste Solid Waste 0uperfund TCLP Compounds ---- . Sample Type Inorganic CompoWlds Results(mg/1) I Environmental Concentrate Comments -arsenic -barium Ground Water (l) Solid (5) cadmium ---chromium -I-Surface Water (2) Liquid (6) lead -- -mercury Soil (3) Sludge (7) -selenium --L silver - Other (4) -Other (8) - - I . - Organic Chemistry Inorganic Chemistry - t:arneter Results (mg/I) fieter Results(mg/1~/Jll '.IJ!W Organic Compounds Results(mg/1) P&T:GC/MS antimony L...0.QD"'-----. -benzene Acid: BIN Ext. --J.-,-"1'senic 40-0 l -carbon tetrachloride - 2A-D --I-barium .!.a.I ____ ,, chlordane I= -----·· ---· ... "". ·········-·--- 2,4,5-TP(Silvex) _ beryllium -chlorobenzene chlordane · ~mi um .L. Q.<?o.5._ -chloroform _ heptachlor . chloride o-cresol --· 1:= hexachlorobenze□ e ~omium <.a.QI -m-cresol hexachlorobutadiene ~alt p-cresol - endrin per L..o.o'5 cresol --l= lindane fluoride 1,4-dichlorobenzene -- methoxychlor iron 1,2-<lichloroethane --_ 'toxaphene ~ad L..D.CIO=:, -1, 1-dichJoroethylene I= -manganese -2, 4-dichloroetbyle□e ~ercury ~0-QOO ..5 -heptachlor ~eke! .!.O-o\ hexachlorobenzene --. nitrate hexachlorobutadieae l-~enium -L...c_.-;,a.5 ~ bexachloroethane -~Iver .!. C ~ ;5;;! "', -methyl ethyl ketone FOR LAB USE ONLY sulfates nitrobenzene -- lnate Received thallium pentachloropbenol --van.idium pyridine --~zinc <~.cl;J -tetrachloroethylene .Date Extracted -pH -trichloroethy Jene conductivity 2,4,5-trichlorophenol --Date Analyzed TDS 2, 4, 6-trichl orophenol -- -flash point -vinyl chloride .Reported By endrin . ·-- --lindane I Date Ro°f1121 ~UC 17~6 --methoxychlor --toxaphene Lab Number 2,4-D -- --2,4,5-TP (Silvex) I DHS 3191 (Revised J~/93) ll 1 NC Dcpa~ment of .~Viionmcnt, II Hc..ahh, & NaOJ['I.J Ruourcc.s S!)lid Wane Management ~ivi,ion SAMJ'LE Al'IALYSIS REQUEST St.ate Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. · Ralcit:h, North Cuolina 27611-8047 Sample Type I Environmental Concentrate L .- Ground Water (I) Solid (5) Surface Water (2) Liquid (6) Soil (3) Sludge (7) Other (4) Other (8) Organic Chemistry P&T:GC/MS Acid:B/N Ext. 2,4-D 2,4,5-TP(Silvex) chlordane heptachlor hexachlorobenzene Results (mg/I) ------ hexachlorobutadiene ::...._ ____ _ endrin lindane rnethoxychJor toxaphene Comments Inorganic Chemistry Par~eter Results(mg.11)181 II• ~ antimony L_ o O al.a. -i.---"1'senic ~ o -o I -h--,),ari um ,<, c, • l _ beryllium --V""11mium Zo. oq 5 chloride ~orniurn O • .o I ~~:r -<-a .. oF.5 fluoride iron ~ad L.Q.,ao5 _ manganese ______ _ ~ercury :<, 0 D <.>O 5 ~eke! z.o_q I nitrate ~enium '-----------------1 ~ver L-o-oc,S -<'._O,o5 l FOR LAB USE ONLY ate Received ---------- rate-Extracted _________ _ Date Analyzed ________ _ .Reported By • Date ReJ?.orted , l .1 ~ B u1.1i22 ~UC , Lab Number IDHS 3191 (Revised 12(93) sulfates thallium vanadium ___LC"'zinc pH conductivity ______ _c_ TDS flash point ______ _ Inorganic Compounds arsemc barium cadmium chromium lead mercury selenium silver Results(mg/1) Organic Compounds Results(mg/1) benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol p-w:sol cresol 1,4-dichlorobenzene 1,2-dichloroethane 1,1-dichloroethylene ______ _ 2,4-dichloroetbylene ______ _ heptachlor hexachlorobenz.ene hexachJorobutadierie ~ hexachloroetbane methyl ethyl ketone nitrobenz.ene pentachlorophenol pyridine tetraChloroe"tbylene trichloroethylene ------- 2,4,5-trichloropheriol ______ _ 2,4,6-trichlorophenol ______ _ vinyl chloride endrin lindane methoxychlor toxaphene 2,4-D 2,4,5-TP (Silvex) 11 ·, NC Dep"rtmcnt of Environment, SAMPLE Ai'IALYSIS REQUEST St.ate Labon.lOry of Public Hulth P.O. Box 28047, 306 N. Wilmington St. IJ Hullh, & Nawral Ruourccs Solid Wute Management Divi,ion Ralcii;h, North Carolina 2761 l-&047 li~Num'b· er /Jc O (20 I (oo{p 2,<1J Sample ID Number/ C0~020-GW 08/13/98 0935 GRAB _J.:,'...1<::-"'--.lL\.LL.li<lL"'-""''-'-'----='----12345678 -CD081098, NC o: WILSON NamcofSi~ Ccidex Dn.nn s, ·fe..--Coll,,,;tedBy_. __ . liteu,c;ition Q_ x -b_ r,;~ I\}~ Da~ Collected !NORG-CLP HETALS Ground Water I rgency: Hazardous Was~ Solid Was~ _0uperfund TCLP Compounds ---- Sample Type. Inorganic Com pounds Results(mg/1) 63 I Environmental Concentrate Comments -arsenic barium - Ground Water (1) Solid (5) cadmium --"\ -chromium -I-Surface Water (2) Liquid (6) lead -- -mercury Soil (3) Sludge (7) selenium --- L silver -Other (4) -Other (8) - - I - Organic Chemistry Inorganic Chemistry - tameter Results (mg/I) ~eter Results(mgin@: 2L Organic Compounds Results(mg/l) P&T:GC/MS antimony L.... o.oc,/..o benzene - _ Acid:B/N Ext. _J,...,-'lf seni c <....D.-Q I -carbon tetrachloride I= 2,4-D -----------·-· I _ L.--,bl<l:ium ----CJ-_+-, ___ , ____ chlordane . ---- 2,4,5-TP(Silvex) _ beryllium -chlorobenzene chlordane ~dmiua:i Lo.c.o5 chloroform - heptachlor . chloride o-cresol --C hexachlorobenzene ~omium L.,0.0 I rn-cresol - hexachlorobutadiene ~alt p-cresol - -endrin per L. ,o. 95 cresol - I: lindane -fluoride 1,4-dichlorobenzene - methoxychlor -iron 1,2-dichloroethane - -toxaphene ~ad .:..Q. o~s -1, 1-dichloroethylene I -manganese -2, 4-dichloroethylene ~ercury -<:..Q OoQ=i -heptachlor ::Vnickel C .. 19 hexachlorobenzene -- nitrate hexachlorobutadiene J-~enium - L..O-c.a5 ~ hexachloroethaoe - ~Iver L.Q ,~i; -methyl ethyl ketone FOR LAB USE ONLY ·-sulfates nitroben.zene -I Date _Received . -thallium pentachlorophenol -vanadium pyridine -~Zlllc LQ.c5 -tetrachloroethylene 1 Date Extracted -pH trichlor?ethylene - -conductivity -2,4,5-trichlorophenol Date Analyzed -TDS 2,4,6-trichlorciphenol - -flash point -vinyl chloride I Reported By ~ -endrin --lindane Date Roff 2-; ~UG 1796 -methoxychlor -I .~tu -toxaphene -Lab Number 2,4-D -- --2,4,5-TP (Silvex) I DHS 3191 (Revised 1:.193) . NC Depanmcnt of Environment, m' ' SAl\.{PLE AL'IALYSIS REQUEST StAte Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Hullh, & Narural R~ourccs Solid Wutc Management Divi,ion Ralci~h. North Carolina 27611-8047 .:•tteN __ umber_ Alt O (!)0 I (oQw 2.<1J SampleIDNumbe CD-025-5W 08/10/98 1615 GRAB II 12345678 CD08!098, NC · O; WILSON ·Name of Site 1-t Lo t' Cri 51°( 'I, Doi 01 5 I -f6--: Collected By_ / !NORG-CLP {) y_ -b. ) tJ G D teC II ted I e ca ton CG a o ec I ---·· lgency_: Hazardous Waste Solid Waste _0uperfund ---- Sample Type I Environmental Concentrate Comments -Ground Water (I) -Solid (5) ._ Surface Water (2) -Liquid (6) r Soil (3) Sludge (7) - -Other (4) -Other (8) I Organic Chemistry Inorganic Chemistry [arameter Results (mg/I) ~eter Results(mg/l'r:111 ii J;. _ P&T:GC/MS antimony L_ Cl -C c::,u;, Acid:B/N Ext. --J.----"1'S eni C L..<J.cl I= 2,4-D . _ :,.)>«ri um h-Cl.-I-·-····-- 2,4,5-TP(Silvex) _ beryllium _ chlordane . ~mium z,Q.Qo5 _ bepLacblor -chloride I= hexachlorobenzene ~omium 40-Q I _ hexach!orobutadiene ~alt endrin per .z{) .o:.5 I lindane fluoride - methoxychlor -iron toxaphene ~ad "-04,o,o5 I -manganese ~ercury L.. Q ,;:i QQ 5 -~eke! .<'... 0 -:Q I l-nitrate ~enium L_ Q -Q Q ,, ~ver LQ-0 5 FOR LAB USE ONLY sulfates· - IDate Received -thallium vanadium -..k::"'Zinc -<-o.~5 I Date Extracted -pH -conductivity Date Analyzed -TDS. I Reported By -flash point - -Date ReP.orted . · -I 011124AUG1798 -Lab Number - -I DHS 3191 (Revised 1'1/93) KEiALS Surface· Water 86 . .. .. TCLP Compounds Inorganic CompoW1ds Results(mg/l) arsenic -barium -cadmium -chromium -lead - -mercury selenium -silver - - - - - Organic CompoWlds Results(mg/1) benzene -carbon tetrachloride -chlordane ------------cWorobenzene - chloroform - o-cresol -m-cresol - -p--cresol cresol - -1,4-dichlorobenzene 1,2-dichloroethane - -1, 1-dichloroethylene -2, 4-d ichloroetby lene -hepLachlor bexachlorobenzene -hexachlorobutadiene - ~ bexachloroethane - -methyl ethyl ketone nitrobenzene - -pentachlorophenol -pyridine -tetraChloroethylene -trichloroethylene -2 ,4,5-trichlorophenol -2,4,6-trichlorophenol -viny I chloride endrin -lindane - -methoxychlor -toXaphene 2,4-D - -2,4,S~TP (Silvex) . I} 'NC Dq:,a'rtmcnt of Environment, IJ Health, & Nawn.I Rca;ourccs Solid Wane Marugcmcnt Divi,ion SM1PLE Al'lALYSIS REQUEST State Labontory of Public Hulth P.O. Box 28047, 306 N. Wilmington St. Raleigh, North Carolina 27611-R047 . •N~~be~ NameofSite Cri dex. lteLoc.ation /iltoaol foo(p 2.<V SampleIDNumber/N •. CD·Ol6·SW 08/10/98_1615 GRAB--.. .· . . . . . 12345678 CD081098' NC D. WILSON :Yt.1.,,,, 5, ·fe-. Collected By __ ~ .,., · !NORG-CLP {)_ 'i fr;_ r✓-j tJ ~ Date Collected METALS Surface Water , -93 j --···-.. -·. rency: Hazardous Waste --Solid Waste _0uperfund TCLP Compounds -- Sample Type Inorganic Compounds Results(mg/1) I Environmental Concentrate Comments arseruc -barium - Ground Water (I) Solid (5) cadmium --- I-chromium - Surface Water (2) Liquid (6) -lead - -mercury Soil (3) Sludge (7) -selenium .---silver Other (4) Other (8) --- -I -Organic Chemistry Inorganic Chemistry - l:ameter Results (mg/I) fieter Results(mg/1) Ill 'I M Organic Compounds Results(mg/1) P&T:GC/MS antimony L._ 0 • <'.::>Q l.:, -benzene -Acid: BIN Ext. -J,..,,-"1'S eru C L. o .CJ I carbon tetrachloride - I= 2,4-D --l--.J,,rti•1m -~ Q-I ---chlordane -·-·-·---- 2,4,5-TP(Silvex) _ beryllium -chlorobenzene chlordane ~drr.ium <-CJ.,005 chloroform -, - heptachlor chloride o-cresol J= -- hexachloroberuene ~omium ..(. o . o I -m-cresol hexachlorobutadiene ~alt p-cresol -- endrin per L..o.o5 cresol -'= lindane fluoride 1,4-dichlorobenz.ene -- me1hoxychlor -iron -1,2-dichloroethane -toxaphene ~ad L..n. ~a5 l, 1-dichloroethylene - I= -manganese -2 ,4-d ichlo roetby lene ~ercury A-Q,.OQQ5 beptachlor --~ckel 4"..o,DI hexachlorobenzene - I=. nitrate hexachlorobutadiene __0lenium - L.Q.0.:2.5 ~ hexachloroethane -~ver .<'...O .Q 5 -methyl ethyl ketone FOR LAB USE ONLY sulfates nitrobenzene --·late Received -thallium pentachlo_rophenol - -vanadium pyridine - ~c L. o.c5 tetraChlaroethylene . - (ate Extracted pH trichloroethylene -- -conductivity -2,4,5-trichlorophenol ate Analyzed -TDS 2,4,6-trichlorophenol - teported By -flash point -vinyl chloride ·---endrin lindane --Date Reported -methoxychlor l 011f2j ~UC 17'JB - --toxaphene b Number • 2,4-D -- --2,4,5-TP (Silvex) r HS 3191 (Revised 12/93) 11 . -NC nCFah~·.ent of En".if'Onmcnt, IJ .. Heallh,··&. Nawral Resources SAMPLE ANALYSIS REQUEST St.ate Laboratory of Public He.a.Ith P.O. Box 28047, 306 N_. Wilmington St. , Solid w&,ttM.i.iu&cmCflt Divi,ion Ralei1:h, North Carolina 27611-8047 1615 GRAB . 0. WILSON Surface Water 100 ) I ---- -_0uperfund TCLP Compounds 'ency:. Hazardous W a,te --Solid Waste -- Sample Type Inorganic Compounds Results(mg/1) I Environmental Concentrate Comments arsenic - -barium Ground Water(!) Solid (5) -cadmium --chromium I-- Surface Water (2) Liquid (6) lead ---mercury Soil (3) Sludge (7) -selenium -I silver - Other (4) Other (8) --- I Organic Chemistry Inorganic Chemistry - tameter Results (mg/I) ~eter Results(mg::)ll!Q 'I !!lo Organic Compounds Results(mg/1) P&T:GC/MS antimony L..Q .:;;, d,;i. -benzene Acid:B/N Ext. -J.-,-"fsenic Lo .. aJ carbon tetrachloride -- I= 2,4-D --1,.,..b«ti um -·L. .a_,_l_ __ .. --chlordane -2,4,5-TP(Silvex) _ beryllium -cblorobenzene chlordane ~mium L.O 005 chloroform -- beptacblor . chloride o-cresol F -- hexachloroben.zene ~omium L.e;. • c::> l -m-cresol hexachlorobutadiene ~alt p--cresol - -endrin per L..a -a 5 cresol -1=· lindane fluoride 1,4-dichlorobenzene -- methoxychlor· iron 1,2-<licbloroethane -- -toxaphene ~ad L.Q. aa =i -I, 1 -dichloroethylene I= -manganese -2,4-<lichloroetbylene ~ercury L.o ==o.S -beptachlor eke! L.o -ol hexa.chloroben.zene -- . nitrate bexachlorobutadiene 1=· 0Jenium -.L...o -cc,5 ~ bexachloroethane -~ver -<:.o :a5 methyl ethyl ketone -FOR LAB USE ONLY sulfates nitroben.zene --late. Received thallium pentachloropbenol -- -vanadium pyridine - ~zinc L. 0-05 tetrachloroetbylene - (ate Extracted pH trichloroethylene -- -conductivity -2,4,5-trichlorophenol ate Analyzed TDS 2, 4, 6-trichlorophenol -- -flas.h point -vinyl chloride feported By -endrin ·-lindane -- Date ReP,031 --methoxychlor I O _ 126 AUG 1798 --toxaphene ...ab Number 2,4-D -- --2,4,5-TP (Silvex) DHS 3191 (Revised l::!/93) I NC Depanmcnt of Environment, E' ' SMIPLE Ai'IALYSIS REQUEST · State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Hc.ah.h, &. Narural Ruourccs Sofid Wut.c Muugcmcnl Divi,ion Ralcii;h, North C.1rolin1 27611-8047 lttc Num. ber ...,M"'-->,to<:..>,o'-"'o-"'o'-'l_(o""'-"'o .... w._,,::2o...c,u51_1J=---Sample ID Numb, C0-030-GW 08/11/98 1705 GRAB IJ -12345678 C0081098, NC 0. WILSON NameofSite Cri dex Da✓ m s I ·fe...;.-Collected By_·_ II ' j !NORG-CLP METALS Ground Water llitel.oC-'tion {))(lo C(.i) /t/ C,, Date Collected __________ .. =-1_0_4_~-----=====-· __ Solid Waste _0uperfund TCLP Compounds H=dous Waste Sample Type 1· Environmental Concentrate -Ground Water(!) -Solid (5) l-Surface Water (2) -Liquid (6) .-Soil (3) -Sludge (7) Other (4) Other (8) -- I Organic Chemistry rara;irGC/MS r~-Acid:B/N Ext. I= 2,4-D 2,4,5-TP(Silvex) I chlordane heptachlor Results (mg/1) = hexachloroben.zene hexachlorobutadiene~----- endrin ~ :::ychlor toxaphene ------ FOR LAB USE ONLY IDate Received _________ _ .Date Extracted _________ _ Date Analyzed _________ _ .Reported By Date~ef°fi27 AUG 1798 ILab Number I DHS )[91 (Revised 1219)) Comments Inorganic Chemistry Par";Jleter Results(mg/l'lft 1i·1? _Lantimony L..O,.ac,(q. -l,.,--"1'S e ni C ---J_,.)>atium _ beryllium ~mium chloride L...o ooS: ~omiurn L.:. O , a l ~~r L...Q-Cl5 fluoride lron L...0-005 _ manganese ______ _ · ~ercury ,(_ D • c AO 5 ~eke! L. c • O l nitrate ~enium ~ver sulfates thallium vanadium - <-c-005 L...o. o5 ..k'.:"""'zinc L... o • q .5 . -pH _ conductivity ______ _ TDS (las.h p(?int ______ _ Inorganic Compounds arseruc -barium -cadmium -chromium -lead - -mercury selenium -silver - Organic Compounds benzene carbon tetrachloride -chlordane Results(mg/1) Results(mg/1) -·-·-·· -·-·-·--------chlorobenzene - chloroform -o-cresol -m-cresol - -p-cresol cresol - -1,4-dichlorobenzene -1,2-dichloroethane -l, 1-dichloroethylene -2, 4-dichloroethylene -heptachlor hexachlorobenzene -hexachlorobutadiene -~ hexachloroethane _ methyl ethyl ketone nitrobenzene --pentachlorophenol -pyridine -tetraChloroethylene -trichloroethylene -2,4,5-trichlorophenol -2,4,6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -loxaphene 2,4-D - -2,4,5-TP (Silvex) NC Depa"mcnt of Environment, Hc.illh, &. Nawral Reiourccs Solid W1_,~ Management Divi,ion SAL\1PLE Ai'l'ALYSIS REQUEST St.ate Laboratory of Public Hu.Ith P.O. Box 28047, 306 N. Wilmington St. Raleii;h, North Carolina 27611-&047 1i~N~~~ .. :f}t(4' 0 t'JOJ (oOw J.<1J. ·.· . Name of Sile: Cridex .. Drum s I :t~ Collected By_·_ liteLoc:ition Q )( & C(,j. tJ <'.:c Sample ID Number/ ·CD-031-GW 08/11/98 .. 1850 .. GRAB 12345678 CD081098, NC D. WILSON !NORG-CLP NETALS Ground Water ' -·------~ . rgency: Hazardous Waste Solid Waste _0uperfund TCLP Compounds ---- Date Collected 108 Sample Type Inorganic Com pounds Results(mg/1) I Environmental Concentrate Comments arseruc - -barium Ground Water (1) Solid (5) cadmium --- L -chromium Surface Water (2) Liquid (6) -lead --mercury .--Soil (3) Sludge (7) -selenium -silver - -Other (4) -Other (8) - -f - Organic Chemistry Inorganic Chemistry - IPararneter Results (mg/I) ~eter Results(mgll)=,:g ii g) Organic Compounds Results(mg/1) P&T:GC/MS antimony L.0_09<..i:, benzene - -Acid:B/N Ext. -J..,-"1'S e ru C <0.01 carbon tetrachloride - I 2,4-D ----------·· -j;_.),ati um _L.. ~ l ,, ___ ---chlordane -- 2,4,5-TP(Silvex) _ beryllium -chlorobenzene -chlordane . -V"'1°mium L..0.005 -chloroform I heptachlor -chloride o-cresol - hexachlorobenzene ~omiurn L.o. o 1 m-cresol - hexach.lorobutadiene ~alt p-cresol -- endrin per L-.o ... 65 cresol I - lindane fluoride 1,4-dichlorobenzene --I -methoxychlor iron 1,2-dichloroethane -- -toxaphene ~ad L.0. c,D5 · -l, 1-dichloroethyleoe I --manganese 2, 4-dichloroetbyleoe -•-~ercury ..:'..0-0oc,5 heptachlor - -~eke! L. 0 • !:2 J -hexachlorobenzene l-nitrate hexachlorobui.adiene ~enium - L..Q "G3 ~ hexachloroethane - ~Iver L. C, -Q s -methyl ethyl ketone FOR LAB USE ONLY -sulfates n.itrobenzene I Date Received thai'lium ---pentachlorophenol vanadium pyridine -~c L.Q_c5 -tetrachloroethylene I Date Extracted -pH trichJoroethylene - -conductivity -2, 4, 5-tri chlorophenol Date Analyzed -TDS 2,4,6-trichlorophenol -I Reported By -flash point -vi.nyl chloride endrin .. ~ -lindane -- Date Re0orted methoxychlor I t1i2tl AUG 17~B -- --toxaphen~ uib Number 2,4-D -- --2,4,5-TP (Silvex) I DHS 3 I 9 I (Revised l"~/93) I NC o.:Partmcnt of Environment, Hc.&llh, &. Natural Ruourccs Solid Wu1.e Managemcnl Divi,ion SAMPLE Ai'l'ALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Ralcii;h, North Carolina 27611-&047 liteNum~~r Alt O rpo / (oofo J.<1J Sample ID Number,. C0"032-PW 08/13/98 .. 1308 GRAB . 12345678 CD081098, NC D. WILSON Name of Site . Ori £ex . f)a; m 5, ·te....--: Collected By_·_.-· PQJJIBL.E WELL_:__ I /). J , / !NORG-CLP METALS Ground Water 112 iteLoc.:,tion /) )( tf2 CC,) (V Cc Date Collected \ tgency: HSazaramdpoluse TyWasptee I Solid Waste 0uperfund·-•----.=-~--'-'-=-=----'--'T=CccL_P_C_o_m_p_o;...u_n_ds ___ ::.;::_, I~ Inorganic Compow11ls Results(mg/1) I Environmental Concentrate Comments arsenic barium \_ Ground Water (1) Solid (5) cadmium L chromium Surface Water (2) Liquid (6) lead I • Soil (3) Other (4) Sludge (7) Other (8) Organic Chemistry ··rararneter P&T:GC/MS ,- Acid: 8/N Ext. 'I= 2,4-D 2,4,5-TP(Silvex) I-chlordane I= heptachlor hexachlorobenzene ,_ hexachlorobutadiene endrin I= lindane methoxychlor toxii.phene Date Received Results (mg/I} ---------- .Date Extracted _________ _ Date Analyzed _________ _ .Reported By I Date Rcr~~fi2'.3 AUG 1 '7 ~8 Lab Number IDHS 3191 (Rcvi,ed 11193) Inorganic Chemistry mercury selenium silver Par~eter Results(mg/l)(ll • Organic Compounds ..'L antimony .£..o ·"' o~ benzene Results(mg/1) -J,.,---"1'senic L.. o . 0 l carbon tetrachloride ·-¾,.,.barium . ~-o •. l --·---. _ beryllium ~dmium Z Q ., po 5 chloride ~omium L. Q , o l -c,99aJt _JC'copper L.o.o5 fluoride iron ~ad _ rrunganese ______ _ ~ercury ~eke! nitrate ~en.ium ~ver sulfates thallium vanadium ~inc pH L...o .:.;;;,s;,a5 L...c:,,.ol L..o.o5 conductivity -------TDS flash point ------- chlordane chlorobenzene chloroform o-cresol m-cresol p-cresol cresol 1,4-dichlorobenzene -------1,2-<lichloroethane 1, 1-dichloroethylene -------2, 4-dichloroethylene -------beptachlor hexachlorobenzene hexachlorobutadiene ~ bexachloroethane methyl ethyl ketone nitrobenzene pentachloropbenol pyridine tetrachlor·Oethylene trichloroethylene 2,4,5-trichlorophenol ------- -------2,4,6-trichlorophenol ______ _ vinyl chloride endrin lindane methoxychlor tcixaphene · 2,4-D 2,4,5-TP (Silvex) I ' NC o,i,rtm,nt of Environmont, Hc.ail.h, & Na.rural Resources Solid Wut.e Management Divi,ion SAMPLE Ai'IALYSIS REQUEST State LaboralOry of Public Health P.O. Box 28047, 306 N. Wilmington St. Raleigh, North Carolina 27611-8047 liteNumber /JC, O (20 I (oow 2,\,0 . Sample ID Number/N, C0-019-SW 08/13/98 1530 GRAB . 12345678 C0081098, HC O. WILSON - DOWNGRAOIENT FROK WETLAND -rameofSite Sitel.oc:1tion Cci dex tJa,, m S ,·fe.----Collected By __ [) x-&J_ ,,J !NORG-CLP-· METALS Surface Water -· Date Collected 129 ) I lgency: _0uperfund Hazardous Waste Solid Waste TCLP Compounds ---- I Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments -arsenic barium -.-Ground Water(!) Solid (5) -cadmium --chromium Surface Water (2) Liquid (6) lead --- -mercury •-Soil (3) Sludge (7) -selenium --silver Other (4) -Other (8) - n - - Organic Chemistry Inorganic Chemistry -· arameter Results (mg/I) ~eter Results(mg/-•= 'I a~ .. Organic Compounds Results(mg/1) -P&T:GC/MS antimony L..c,. o=<..a beI11.ene -I= Acid:B/N Ext. --l,./"tsenic L..0.01 carbon tetrachloride -· 2.,4-D --· ------.. -·-L.--··ba.ti.um .. L.. 0 -) _________ , .. chlordane ---- _ 2,4,5-TP(Silvex) _ beryllium · -chlorobenzene . chlordane . ~mium L..o. co~ chloroform --E hcptachlor -chloride -o-cresol hexachlorobenz.ene ~omi urn 0-01... m-cresol - hexachlorobutadiene ~alt p--cresol - I endrin pper <J -\ y cresol - lindane fluoride 1,4-dichlorobenz.ene --· -methoxychlor -iron 1,2-<lichloroethane - I loxaphene ~ad .(o -00$ 1, 1-dichloroethylene - -manganese -2, 4-dichloroethylene -~ercury .<:..c • .qco5 heptachlor - I -:Vnickel 0 -Q9 -hexachlorobenzene -nitrate hexachlorobutadiene ~eniurn - L ,o_c,95 ~ hexachloroethane - ~ver L..c, -Q 5 -methyl ethyl ketone ·I FOR LAB USE ONLY -sulfates nitrobenzene .- -thallium · penta~hlorophenol - Date Received -vanadium pyridine -I Date Extracted ~nc Cl -ii -tetraChlo_roethylene -pH -trichJoroethylene conductivity 2, 4, 5-trichl orophenol -- Date Analyzed -TDS 2, 4,6-trichlorophenol I Reported By - -flash point -vinyl chloride -endrin -lindane --I Date Rf orted methoxychlor . 0 .1131 ADGl798 -- --toxaphene Lab Number 2,4-D --I p11s 3 I 9 I {Revised l ::2/93) --2,4,5-TP (Silvex) I NC Dep,~m,nt ofEnvironm,nt, Si\illLE Ai"l'ALYSIS REQUEST Stat< ubontory of Public He.,lth Hu.llh, & N1.rural Ruourc:c, P.O. Box 28047, 306 N. Wilmington St. Solid Wute Management Divi,ion Ralci~h. North Carolina 27611-8047 'Number Alt O (20 I (oo(o ci ,<1J Sample ID Number CD·D28::GW _ 08/12(.98 1205 GRAB · ••· ~·"· · • · 12345678 CD081098, NC · D. WILSON [ eofSite Loc:ition Crisfex <tJo, 01 ,5 ,'fC= CallectedBy_·_ PERHAN_ENT: __ HONITORJNG WELL /) J tJ ~ !NORG-CLP HETALS Ground Water I ---· ... ------133 {) 'I. t1}. r {,) 0 Date Collected lency: Hazardous W a.ste Solid Waste _0uperfund TCLP Compounds ---- · Sample Type Inorganic Compowu!s Results(mg/1) .Environment.al Concentrate Comments arsenic -barium - Ground Water (I) Solid (5) cadmium --I -chromium Surface Water (2) Liquid (6) -lead --mercury t Soil (3) Sludge (7) -selenium -silver - -Other (4) -Other (8) - I - - Orgartic Chemistry Inorganic Chemistry - Results (mg/I) ~eter Results(mg/1) . Organic Compounds Results(mg/1) .1TT1eter P&T:GC/MS . antimony L.O Q o<'..a, benzene - Acid:B/N Ext. -i,,-arsenic L..c OJ carbon tetrachloride f _.; __ a.,,. I -2,4,D -~um chlordane ·-----·----·-··-·-·- 2,4,5-TP(Silvex) _ beryllium -chlorobenzcne chlordane . ~mi um L.Q 005 chloroform --t beptachlor -chloride -o-cresol hexachlorobenzene ~omium L..Q. al m-cresol - -hexachlorobutadiene ~all p-cresol - I= endrin pper· L....Q.CJ5 cresol - !ind.me fluoride 1,4-dichlorobenzene -- methoxychlor· iron 1,2-<lichloroethane --- toxaphene _0ead "'-0 005 I, 1-dichloroethylene a= -_ manganese -2,4-dichloroethylene ~ercury L....Q • Q ~21::i _., beptachlor -- -~eke! <-Q-<;,I -hexachlorobenzene I-nitrate hexachlorobutadiene . ~enium -L...o-=oS ~ hexachloroetbane - ~ver L..a. a5 -methyl ethyl ketone ' FOR LAB USE ONLY -sulfates nitrobenzene thallium - --pentachloropbi:nol ate Received vanadium pyridine --...J,c'zinc --<'.. 0. C> .!, tetrachloro~thYlene late Extracted - -pH trichloroethylene - -conductivity -2,4,5-trichlorophenol Date Analyzed -TDS 2,4,6-trichlorophenol - leported By -flash point vinyl chloride - ·----endrin lindane -- (le RQ'fl'l32 ~UG 1798 --methoxychlor toxaphene -- b Number 2,4-D -- -2,4,5-TP (Silvcx) HS 319! (Rcvi:;cd 1:2/93) -I I ' ' NC Department of Environment, He.a Ith, &. Na rural Ruources. Solid Wute Man.a1:emcnt Divi,ion SAi\1J'LE A.t'1ALYSIS REQUEST State Labontory of Pubtic Health P.O. Box 18047, 306 N. Wilmington St. R.alei~h. Nonh Cuolina 27611~8047 litet:l~~ber !IC-0 (20 I (oo(p 2,<1J Sample ID Number, CD-029-GW 08/12/98 1510 GRAB · 12345678 C0081098, NC D, WILSON PERMANENT KONITORING WELL · lfameofSite . ~itel..ocation !NORG-CLP KETALS Ground Water Date Collected 137 I lge□cy: · Hazardous Waste Solid Waste 0uperfund TCLP Compounds ---- I Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments arsenic -barium - Ground Water (1) Solid (5) cadmium .--- -chromium Surface Water (2) Liquid (6) -lead --mercury t-Soil (3) Sludge (7) selenium -- -silver -Other (4) -Other (8) - J - - Organic Chemistry Inorganic Chemistry - farameter Results (mg/I) ~eltt Results(mg/l)(S g 'I gi,. Organic Compounds Results(mg/1) P&T:GC/MS antimony L..o_c.o<:c -benzene Acid: BIN Ext. ---v-"1"'enic .<'... O.Q l -carbon tetrachloride u== 2 4-D _ -~ um _.,(_c, ... , chlordane -------------·-··--·---_ 2,4,5-TP(Silvex) _ beryllium -chloroben.zene -chlordaoe . ~mium ,t.__ Q -.cia l:, -chloroform ~ beptachlor chloride o-cresol --hexachlorobenzene ~mium L..Q~ol -m-cresol -bexachlorobutadiene ~~t· p-cresol - I= endrin per LQ-D la; cresol -lindane fluoride 1,4-dichlorobenzo□e -- -methoxychlor iron 1,2-dichloroethane -- I toxaphene ~ad L..Q _CJQ 5 -I, 1 'dichloroethyle□e -manganese -2, 4-dichloroetb y I ene ~en:ury .ZO,CJODD heptachlor --eke! L_. o .c, I bexachlorobenzene -I nitrate hexachlorobutadiene ~enium --<-o-c3 ~ bexachloroetbane - ~•er "--O. o5 -methyl ethyl ketone I FOR LAB USE ONL y sulfates nitrobenzene --th~lium pentachlorophenol --Date Received vanadium pyridine - .Date Ex"tracted ..J.c"'zinc -t__ c .as -tetraChloroetb y lene -pH trichloroethylene conductivity -2, 4, 5-trichlorophenol --Date Analyzed -TDS 2,4,6-trichlorophenol -I Reported By -flash point -vinyl chloride .--endrin lindane --I Date Reported --methoxychlor 011133 AUG 1798 --toxaphene Lab Number · 2,4-D -- -2,4,5-TP (Si]vex) DHS 3191 (Revised 11/93) -I I 'NC Dcp;rtm,nt ofEnv;ionm,nt, SMIPLE ANALYSIS REQUEST St.ot< ubontory of Public Heolth Hullh, & Nawn.I Ruaurcc:s P.O. Box 28047, 306 N. Wilmington St. Solid Wane Marull;cment Division Ralcii:h, North C1.rolina 27611-8047 •~Number !Ito (20/ (oo{o :1.<V Sample!DNumb, C0-040-SW 08/13/98 1625 GRAB ,:-,,, · • 12345678 ·CD081098, NC D, WILSON ·c· eofSi~ 1teLoc:ition Cr; d-ex · Do✓ m S, ·fe...---Collected By_·_·· .. . j !NORG-CLP {) 'i bJ_ re; tJ {!,,,, Da~Collected · . ' METALS Surface Water . . 141 J Jency: _0uperfund Hazardous Was~ Solid Was~ TCLP Compounds ---- · Sample Type Inorganic Com poWJds Results(mg/1) I En.vironment.aI Concentrate Comments -arsenic barium - Ground Water(!) Solid (5) cadmium r -- -chromium Surface Water (2) Liquid (6) lead -- -mercury t-Soil (3) Sludge (7) selenium --silver - -Other (4) -Other (8) - I - - Organic Chemistry Inorganic Chemistry - farameter Results (mg/1) ~e:er Results(mg/1) 0 § g;.. Organic CompoW1ds Results(mg/1) _ P&T:GC/MS antimony L, 0 -c,c, <;;, benzene -Acid:B/N Ext. ...J.-,-"1'senic -<-<1-0l carbon tetrachloride -·F 2,4-D -------· --~um 4 <J. I -chlordane -·--·----------·- 2,4,5-TP(Stlvex) _ beryllium. -chlorobenzene -chlordane . ~ mi U ID L..Q,<>o.S chloroform -I= heptachlor -chloride -o-cresol hexachloroben.zene ~omium L.o_c,I m-cresol - -hexachlorobutadiene ~alt p-cresol -I= eodrin pper L.q_. of, cresol - lindane ' fluorid~ 1,4-dichlorobenzene ---= methoxychlor -iron -1,2-<lichloroethane toxaphene ~ad -<:.Q -~ ~ -I, 1-dichloroethylene -manganese -2, 4-di chlo roe thy iene -~ercury L...0-Qe>o..=i -beptachlor ~ckel .L.Q.Ql -hexachloroben.zene F nitrate bexachlorobutadieoe ~enium - L.. o cc,o5 ~ hexachloroethane - ~vcr L.. <) -c!!! 5 -methyl ethyl ketone ~ FOR LAB USE ONLY -sulfates nitrobenzene - -thallium pentachlorophenol - ate Received vanadium pyridine - tate Extracted __0inc L..c.s::i5 -tetrachlor?ethylene -pH trichJoroethylene - -Conductivity -2,4,5-trichlorophenol Date Analyzed -TDS 2,4 ,6-trichlorophenol - leported By -flash point -vinyl chloride ··-endrin -lindane · -- (te Reported --methoxychlor . 01.11:3,~ ~OG1798 --toxaphene b Number 2,4-D -- --2,4,5-TP (Silvex) HS 3191 (Revi:;ed l:Z/93) t . _._: I • NC D~~;J,:n,){::rorun,nt, Hc.alr.h,i &. Nawral Ruources Solid Wut.c Management D1vi"on SAMl'LE A.i'l'ALYSIS REQUEST Slate Laboratory of Pub~ic H.;_,.lth P.O. Box 28047, 306 N_ . .Wilmingtori St. Raleigtl, North C.1ro\~a 27611-8047 .. ,.,.~~~~'~f~;~4iq,g_pf£L~P~.?l:£1?... S~lel?~umb ~~;~~~;:e c~~~;~~:~ N~OOOD.c~~rsoN .c,=e~fSiJi~;.;c;;,::ifi'~-/)a;~:'Y5: /fe--< u,ll~t~~y -~~ -!NORG-CLP -METALS ·• Rinsate SiteLoc:ition {) x ·-b,_ ,J /l.} ~ DateCollected -155 ) j .. ---. ~-- lgency: _0uperfund TCLP Compounds Hazardous Waste Solid Waste -- Sample Type Inorganic Compow,cls Results(mg/1) I Environmental Concentrate Comments arsenic -barium - Ground Water (I) Solid (5) c:idmium .--- -chromium Surface Water (2) Liquid (6) lead --- -mercury I-Soil (3) Sludge (7) -selenium -silver - -Other (4) -Other (8) - I - - Organic Chemistry Inorganic Chemistry - farameter Results (mg/I) ~eter Results(mg/1:•ilf§ al Organic Compow,cls Resul ts(mg/1) _ P&T:GC/MS antimony L-o .c;,o<o benzene - I= Acid:B/N Ext. -1,.,--"f S eni C L.O.c,1 -carbon tetrachloride 2,4-D _ I,. )>ati um _-s,Q_. l chlordaoe ---------·-- 2,4,5-TP(Silvex) _ beryllium cWorobenzene - ·chlordane . ~mium LO. D05 -chloroform ~ hepU!chlor -chloride -o-cresol hexachlorobenzene ~omium L..o:QI -m-cresol hcxachlorobutadiene ~alt p-cresol - endrin per -t...o.q';;, cresol - lindaoe fluoride 1,4-dichlorobenze□e -- -methoxychlor iron J ,2-dichloroethane --~ toxaphene __0ad <-o .oo5 -I, 1-dichloroethylene _ mang~ese 2, 4-dichloroethylene - -~ercury ~ o. s;,c c-5 -hepU!chlor ~eke! L...Q.ol hexachlorobenzene F -nitrate hexachlorobuU!diene ~enium -Lo ... o 0 ~ ~ bexachloroetbane - ~ver L.. C . Q Q -methyl ethyl ketone I FOR LAB USE ONLY -sulfates nitrobenzene - -thallium penU!chloropbenol - Date Received -vanadium pyridine - lnatc Extracted ..k::""'zinc L..o .a5 tetraC.hloroCthylene - -pH -trichloroethylene conductivity 2,4,5-trichlorophenol --Date Analyzed TDS 2,4,6-trichlorophenol .Reported By -- -flash point vinyl chloride - ---endrin lindaoe --I Date Reported -methoxychlor 01..ti:t:-J ~UG 1796 - --toxaphene Lab Number 2,4-D --2,4,5-TP (Silvex) DHS 3191 (Revised 1:2/93) --I I ' NC Dq:ianmcnt of Environment, Hc.a!th, &. Natural R~ourccs Solid Wute Marui:'cmcnt Divi,ion SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Ralcii,:h, North Carolina 27611-8047 lite Number Name of Site liteLoc:ition AIC-D (20 I (oo{p 2 ,51) Sample ID Numbe C0-300-0B 08/11/98 1000 GRAB · . .. 12345678 CD081098, NC D. WILSON Cridex Dev tYJ S, ·fe----Collected By_·-·-_ _. I . !NORG-CLP /) Y.. -bJ. '"') A}~ Date Collected KETALS -- - i ---- --- lgency: --Hazardous Waste --Solid Waste _0uperfund TCLP Compounds 156 Sample Type . Inorganic Compounds Results(mg/1) I Environmental Concentrate Comments -arsenic barium - Ground Water (1) Solid (5) -cadmium -- I-chromium - Surface Water (2) Liquid (6) -lead - -mercury Soil (3) Sludge (7) -selenium .-- -silver Other (4) Other (8) --- -f -Organic Chemistry Inorganic Chemistry - F-runeter Results (mg/I) ~eter · Results(mgl";i0. ac. Organic Compounds Results(mg/1) P&T:GC/MS antimony L...,o_ o=l..<:z -benzene Acid:B/N Ext. ---1,.,--"l"senic -<'...:Q ol -carbon tetrachloride I= 2 4-D ~um L.a -l chlordane 2:4,5-TP(Silvex) --_ beryllium -chJorobCn.zene chlordane ~mium .L..c Aa5 chloroform -. - I= heptachlor -chloride o-cresol - hexachJorobenzene ~omium .L....D. ,:, I -m-cresol hexachlorobutadiene ~~t p-cresol - endrin pper L..o-oS cresol -~ lindane fluoride 1,4-dichlorobenzene -- methoxychlor iron 1,2-dichloroethaile -- toxaph~ne ~ad L..o 005 -1, 1-dichloroethylene _ manganese -2, 4-dichloroetb y lene ~ercury L..o_cc,OS: beptachlor - -~eke! ""-o.c 1 hexachlorobenzene - 11-nitrate bexachlorobutadiene ~e~um -Lo ,oo.5 ~ hexachloroethane - ~ver L.0%05 methyl ethyl ketone - FOR LAB USE ONLY sulfates . nitrobenzene -- IDate Re.c"eived -thallium pentachloropbenol -vanadium pyridine -~zinc "'--<0 .o5 -teiraCWoroethylene I Date Extracted -pH trichloroethy lene - -conductivity 2,4,5-trichlorophenol -Date An~yzed -TDS 2,4,6-trichlorophenol -I Reported By -flash point -vi.nyl chloride ---endrin lindane -- Date Re(J°rted. methoxycblor I -1113ti AUG 1798 -- --toxaphene Lab Number 2,4-D -- --2,4,5-TP (Silvex) DHS Ji9I (Rcvi5ed l::Z/93) I • , NC Dcp~rtment of Environment, Heah.h, & Natural R~ourccs Solid Wut.e Management Divi,ion SAMPLE ANALYSIS REQUEST State Laboratory of Public He.allh P.O. Box 28047, 306 N. Wilmington St. Ralcii,:h, North Carolina 27611-8047 lteNumber Alto C)O 1 (oo(p 2:¢1J . >-'Sa_rripl':lDNumb.CD-clOO-PB · ..,...... · ·•. ·. · ......... ,,e,,·,, ... , ..•.. ,.,,:, ,.:·..... , ... , .. ,,,c~,,,',,,.,.:."r·.-,.:-;,.:,". 08/14/98 1300 . Water CD081098 i r~::;:. ~•t~JJ°tL~it~::!:'' ;;.~i~" ,;:::"'";NAalo lgency:. Hazardous Waste Solid Waste _0uperfund TCLP Compounds ISi Sample Type I Environmental Concentrate .-Ground Water (I) Solid (5) Surface Water (2) Liquid (6) t-Soil (3) Sludge (7) Other (4) Other (8) Organic Chemistry f arameter Results (mg/I) _ P&T:GC/MS Acid:B/N Ext. 2,4-D 2,4,5-TP(Silvex) chlordane heptachlor hexachlorobenzene -------hexachlorobutadiene '-------·end rin lindane methoxychlor toxaphene I FOR LAB USE ONL y "r:iate Received _________ _ tale Extracted _________ ~ Date Analvzed Leported ~y ---------- rate Reported . 0111]7 AUG 1798 Lab Number IDHS 3191 (Rcvi!.cd ]'.:./93) Comments Inorganic Chemistry Par";:lleter .Results(mg/1,4!£ ala _1t: antimony L... o _c,p(,,, ~senic Zo .o 1 --t,.)>•rium -~ q "-'''----- -beryllium ~mium <'...,o. ,;;,o 'S chloride ~omium L..O .c:, I _ ':!,l>alt _0opper .L.o_ aS fluoride iron ~ad _ manganese ______ _ ~ercury L...e:i.-00:05 ~ickel "-o . c I nitrate ~enium ~ve.r sulfates thallium vanadium ~c pH ""-o .oo-5 <-.o .• c5 L..o.oS conductivity ______ _ TDS fla.sh point ______ _ Inorganic Com pow,ds arsenic barium cadmium chromium lead mercury selenium silver Organic Compow,ds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m--cresol p-cresol cresol 1,4-dichlorobenze□e 1,2-dichloroethane Results(mg/1) Results(mg/1) I, 1-dichloroethyle□e ______ _ 2,4-dichloroetbylene ______ _ beptachlor hexachloroben.zene hexachlorobutadieoe ______ _ .... bexachloroethane methyl ethyl ketone nitrobeozene pentachlorophenol pyridine tetrachloroeth y lene trichloroethy lene 2,4,5-trichlorophenol 2,4,6-trichlorophenol vinyl chloride endrin lindane methoxychlor toxaphe□ e 2,4-D 2,4,5-TP (Silvex) ------- ------- I 'NC Dcp~rtment of Environment, Hull.h, &. Nawral R~ourccs Solid. Wut.e Man.agement Divi,ion SAMPLE A.t'l'ALYSIS REQUEST SlAtc Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Raleillh, Nonh Carolina 2761 l·R047 _.teNumber /1!;.,Q (20/ (oQ(o fi.<-1J Sample ID Number/I -C0~024-SW 08/10/98 1520 GRAB C,, · 12345678 C0081098, NC D. WILSON lame of Site ~J de y, fJcu m 5 i -fe--, Collected By_·_ !NORG-CLP ri"IJ /·!~ teLoc:ition-ew,!__.).Xs.,ttJµ.,.c.JULi:'.:(,L'J;--,/-/JLIL-~~=----DateCollected _0uperfund Hazardous Waste Solid Waste Sample Type I Environmental Concentrate Ground Water (I) Solid (5) L Surface Water (2) Liquid (6) .-Soil (3) Sludge (7) Other (4) Other (8) Organic Chemistry l ararneter _ P&T:GC/MS Results (mg/I) I- Acid:B/N Ext. 2,4-D 2,4,5-TP(Silvex) chlordane heptachlor hexachloro benzene -------hexachlarabutadiene '------- endrin lindane methoxychlor toxaphene Comments Inorganic Chemistry Par~eter Results(mgil:011 al _x antimony ~ .o _ c,p<.a -J...--""'senic L.. o . Q l --+_pKtium I..... Q_. 1 _________ _ _ beryllium ~dmium L.. O. ,:.:, Q.5_ chloride ~hl-omiurn L.. Q t o \ -"_3l,alt __j,C"copper L....,o _ q 5 fluoride iron L...o-=o5 _ manganese ______ _ ~ercury ~<). 000-2.. ~eke! Zc -Q l nitrate ~eniurn ____________ _;_ __ ~ ~ver L..{)_ 0,05 L.a_,:-,'5 l FOR LAB USE ONLY ate Received _________ _ tate'Extracted _________ _ Date Analyzed _________ _ Jeported By .Date Reo1.1ts7 AUG 1798 Lab Number IDHS 319 I (Revi:.ed 12/93) sulfates thallium vanadium ~nc pH conductivity ______ _ TDS flash point METALS Surface Water 79 TCLP Compounds Inorganic CompoWlds arsenic barium cadmium chromium le.ad mercury selenium silver Results(mg/1) Organic CompoWlds Results(mg/1) benzene carbon tetr.ichloride chlordane chlorobenzene chloroform o-cresol rn-cresol p-cresol cresol 1,4-dichlorobenzene 1,2-dichloroethane I, 1-dichloroethyleae ______ _ 2,4-dichloroethyleae ______ _ heptacWor hex.achlorobenzene hexachlorobutadiene ... bexachloroethane methyl ethyl keione nitrobenzene peatachlorophenol pyridine tetiaChloroethylene trichloroethylene ------- 2,4,5-trichloropheaol ______ _ 2, 4 ,6-tricWorophenol vinyl chloride endrin lindane methoxychlor, toxaphene 2,4-D 2,4,5-TP (Silvex) ------- I· , NC Department of Envil'Onment, SAMPLE ANALYSIS REQUEST SlAte Laboratory of Public Health P.O. Box 18047, 306 N. Wilmington St. Health, & Nawral Ruources R.a!cii:h, Nonh c,.rolina 2761 l·R047 I Solid Wane Managcmcnl Divi,ion SiteNumber /JC, 0 {20 / (oQW J,51) Sample ID Nu· lameofSite Ocidex Do✓m s,-ft::.< CoUectedBy_ C0-004sSL 08/10/98 1345 GRAB 12345678 CD081098, NC D. WILSON SOIL Sitel.oc:ition I))( -lo al tJ C-, DateCol!ectec ■ ) I IHORG°CLP l!Jgency: __ Hazardous Waste Solid Waste _0uperfund I Sample Type Environmental Concentrate I-Ground Water (!) Solid (5) Surface Water (2) Liquid (6) L Soil (3) Sludge (7) Other (4) Other (8) Organic Chemistry arameter P&T:GC/MS Acid:B/N Ext. 2,4-D 2,4,5-TP(Silvex) chlordane heptach!or Results (mg/I) hexachloroben.z.ene _____ _ hexachlorobutadiene'--------- endrin lindane rnethoxychlor toxaphene I FOR LAB USE ONL y Date Received IDate Extracted _________ _ Comments 'P?f:Q le c11n UM:tzl lVli N\ J-r,y, SuspeC-+eJ I Inorganic Chemistry Par'1;!Jleter Results(mg/l)(mg/kg) _L' antimony _.c..-'-.1 ____ _ ---L.,--"l'Senic 1 ~um --~·-· _ beryllium --V"3dmi urn chloride ~omi urn -";lPalt __0opper fluoride iron ~ad ..:.'-l L...10 190 150 l,(J _ m:1.flganese ______ _ ~ercury ..::k-"n i ck e I nitrate ~enium ~ver sulfates thallium Vanadium ..k::""'"z.inc 450 pH conductivity -------TDS HETALS Soil 15 TCLP Compounds Ino~c .Compounds Results(mg/1) ~eruc _,r,"""·•L-L).Q,.,_ ____ _ :::::J>ariurn _ _._,,e..,_I _____ _ yadmiurn -'--D • Q i:::, ".:__,..ehrorniurn L...0.,Q !5 lz: )ead ..L...e,. 05 ~;nerc. ry -"-.0 .QI v Se ruurn .C:.a. o 3 silver ..::_.:, .o,.5 Organic Compounds Results(mg/1) benzene carbon tetrachloride chJ1Jrdan~ chlorobenzene chloroform o-cresol rn-cresol p-cresol cresol 1,4-dichlorobenzer,e ______ _ 1,2-dichloroethane l, 1-dichloroethylene ______ _ 2,4-dichloroelbylene ______ _ heptachlor bexachlorobenzene hexachlorobutadiene . ... hexachlo"roethane methyl ethyl ketone nilrobenzene _p~ntachlorophenol pyridme tetraChloroetbYlene trichloroethylene 2,4,5-trichlorophenol 2,4,6-trichlorophenol ------- ------- -------.Date Analyzed Reported By t:}a5h point -------vinyl chloride I Date l\J'f'ti];J AUG 1798 Lb Number I DHS 3191 (Revised l'.'193) endrin lindane methoxychlor toxaphene 2,4-D 2,4,5-TP (Silvex) I ' NC Department of Environment, Health, & Nawral Ruources Solid Wut.c Marugcmcnl Divi,ion SAMPLE Ai~ALYSIS REQUEST Slate Labon.tory of Public Healr.h P.O. Box 28047, 306 N. Wilmington St. R&lciRh, Nanh Carolina 27611-8047 .lite Number .-'M'-"_'-'C-""''-'OL ___ J..P?,:.lPL_ LI ..IJ(o""Q"'-'-"(p'.....!L:)W,J.<_1J""-. __ Sample ID Numbe CD-033-SL • o~_/12/98 .1545 . GRAB 12345678 CDO81O98, NC D. WILSON SOIL !NORG-CLP HETALS Soil NameofSi~ ()ri dex Dev m s ,-t~ Collected By_·_ lite Location () 'I. -b. ,,J A} C,, Date Collected ) I -··-··--------~--- lgency: --Hazardous Waste --Solid Waste 0uperfund TCLP Compounds 115 Sample Type rzanic Compounds Results(mg/1) I Environmental Concentrate Comments arsenic D, o9 pc(,:Je_td A ✓-barium O _ 9 · Ground Water (1) Solid (5) ~admium L.. C 7 o '5 --1 L f;,· , ~, 0hromium ...(_ a-o.5 Surface Water (2) Liquid (6) ead L.. o. _o5 -W\ JI a,11 ·lJ c:M ~ury LD.ol Si,S!)ec,./c) r-Soil (3) -Sludge (7) lenium L.. o. o.3 I _ silver L..E:J ~ <)~ Other (4) Other (8) --- I - - Organic Chemistry Inorganic Chemistry - ~arameter. Results (mg/I) ~eter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS antunony LI -benzene _ Ac1d:B/N Ext. __i,.-atsenic ..(_ i,.\ -carbon tetrachloride t 2,4-D. ----__ i,,J,,,ti 11 m ___ J.ao.. -chlordane --2,4,5-TP(Silvex) _ beryllium -chlorobenzene chlordane . ~mium L.. 10 chloroform C - ~ heptachlor -chloride o-cresol - hexachloroben.zene ~omi urn ~~~ -m-cresol hexachlorobut.adiene ~alt p-cresol ,38 - endrin pper cresol ~ - lindane fluoride I, 4-dichlorobenzene --rnethoxychJor -iron 1,2-dichloroethane - . toxaph~ne ~ad 5/o 1, 1-dichloroethylene -~ -manganese 2, 4-dichloroeth y lene - ~ere u ry .::.0.08 -heptachlor yi'iicke~ a1o hexachlorobenzene -nitrate hexachlorobutadiene -~eniurn - L.. d,. ~ hexachloroethane· - ~ver L.. IQ -methyl ethyl ketone I FOR LAB USE ONL y -·sulfates nitrobenzene thaliiurn - --pentachlorophenol Date Received -vanadium pyridine ffio -.J.C"Z.inc tetraChloroethylene - .Date Extracted -pH tricWoroethylene - -conductivity 2,4,5-trichlorophenol - Date Analyzed -TDS 2,4,6-Jrichlorophenol - .Reported By -flash point -vinyl chloride ·-endrin -lindane -- .Date Repd11i~.i9 AUG 17~8 --methoxycbJor --toxaphene Lab Number 2,4-D -- --2,4,5-TP (Si]vex) DHS 3191 (Revised 11/93) I I ' ' NC Dcpa:trr:ent of Environment, ·SAMPLE At'l'ALYSIS REQUEST St.ate Laboratory of Public Hulth Hul!.h, & N1rural Resources· P.O. Box 28047, 306 N. Wilmington St. I Solid Wuic Marugcmcnt Divi,ion R1leii:h, Nonh C.1rolin1 27611-8047 "'tcNurnber A/(;, 0 (20 / (oQ{R ;) ,,C:1J Sample ID Nuinbe CD-OOl·SL 08/10/98 1020 GRAB 12345678 CD081098, NC D. WILSON lameofSite. Cci.sfex Dn1 tr) s ,-f~ CollectedBy_i~~~G-CLP METALS Soil SiteLoc:ition {) x-b C{,~ ft) G DateCollecte<l ____ -;:::::=3=====-=-:___:==3====-:., lgeocy: __ . Hazardous Waste Solid Waste 0uperfund TCLP. Compounds I Sample Type · EnvironmenL'll Concentr.ite t Ground Water (!) Solid (5) Surface Water (2) Liquid (6) I-Soil (3) Sludge (7) Other (4) Other (8) Organic Chemistry 3.rameter P&T:GC/MS Acid: BIN Ext. /4."--D 2,4,5-TP(Silvex) ch!ord.Wi! beptachlor h"exachl orobenz.e~1e Results (mg/11 ------hexachlorobut.adiene "------- endri.n lindane methoxychlor toxaphene I FOR LAB USE ONL y Date Received ----------lo ate Extracted _________ _ IDate Analyzed Reported By _________ _ IDate Reported· o ti~:i~-1,-o~A~uc~r~,~95~ Lab Number IDHS 3191 (Rcv;,cd \c/93) Comments Inorganic Chemistry Par~eter Results(mg/l)(mg/kg) _y antimony __ .<:.=-1:,--___ _ ~'::\ ---J,/"1 Se ni C , barium .. -bv'.. _ beryllium. ______ _ ~dmium chloride ~omi um cobalt ~pper fluoride iron ~ad L. 10 '10 _ manganese ______ _ ~ercur; ~ckel nitrate ~eniurn ~vec sulfates thallium vanadium ~zinc pH ,I.._\() bb conductivity ______ _ TDS flash point Inorganic Compounds arsenic barium cadmium chromium le:id mercury selenium silver Results(mg/1) Organic Compounds Results(mg/1) benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol p-cresol cr~sol 1,4-dichlorobenzene ______ _ 1,2-dichloroethane l, 1-dichloroethylene ______ _ 2,4-dichloroctbylene ______ _ hep!achlor hexachlorobenzene hexachlorobutadieoe -------... hexachloroetbane methyl ethyl ketone· ______ _ nitrabeo..zene pentachlorophenol pyridine tetraChlo~oethylene trichloroethylene. 2,4,5-trichlorophenol ______ _ 2,4, 6-trichlorophenol ______ _ viny I chloride endrin lindane melhoxychlor• · toxaphene 2,4-D 2,4,5-TP (Silvex) I ' NC D~artmcnt of Environment, Hulth, & Natural Resource, SAMPLE Ai~ALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Raleigh, North Carolina 27611-8047 Solid Wutc Management Divi,ion liteNumber Alco (20/ (oo{p 2.<1J Sample ID Numl C0-002-SL -os/10/98 1110 GRAB 12345678 CD081098, NC D. WILSON·· SOIL rameofSite. SiteLoc:itioo !NORG-CLP HETALS Soil 6 I -Date Collected lgency: Hazardous w,._,te Solid Waste _0uperfund TCLP Compounds ---- 1 · Sample Type Inorganic Com pounds Results(mg/1) Environmenq! Concentrate Comments -arseruc barium - Ground Water (1) Solid (5) c:i.dmium .--- -chromium Surface Water (2) Liquid (6) le:id --- -mercury I-Soil (3) Sludge (7) selenium --silver - Other (4) -Other (8) - J - - Organic Chemistry Inorganic Chemistry -. [rarameter Results (mg/I) ~eter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) P&T:GCIMS 1tirnony L.. I -benzene I= Acid: !JIN Ext. ___J,.,,-"f Seru C 44 c:irbon tetr.1chloride. -- 1.4-D ... , J>,,rium . ____ 'io __ ·-·-----chlordane ----·-;;.-·beryllium -·-·--····· ··-.. ·--·-·-··-·--- -2,4,5-TP(Silvex) -chlorobenzene chlordane ~dmium 410 chloroform I - heptachlor chloride o-cresol -- hexach..lorobenzene ~omi ~m 4\\:0 m-cresol - hexachlorobutadiene ~alt p-cresol -- I endrin per bb cresol. - lindane fluoride 1,4-dichlorobenzene .-- -methoxycluor iron 1,2-dichloroethane -- I= toxaphi:ne ~ad ~,o l, 1-dichloroethyleoe - -manganese -2.4-dichloroethyleoe -~ercury .L.o.oP, -beptachlor II ~eke! aia bexachlorobenzene -nitrate bexachlorobutadiene ~eniurn -L..;;),_ ~ hexachloroethane -~Iver 410 -methyl ethyl ketone I FOR LAB USE ONLY sulfates nitroben.zene -- -thallium pentachlorophenol -Date Received vanadium pyridine -- _0.inc ,5_t-, tttrachloroethylene I Date Extracted - -pH -trichloroethylene -conductivity -2 ,4,5-trichlorophenol . Date Analyzed TDS 2,4 ,6-trichlorophenol . I Reported By -- -f_la.sh point -vinyl chloride endri.n . --lindane --I Date(fJPfIZif AUG 17~8 --methoxychlor --toxaphene Lib Number 2.4-D --I DHS 3191 (Revised 12/93) --2,4,5-TP (Silvex) I I ' NC D~ar1mcnt of Environment, Hullh, & Nawral Ruourcc• Solid Wui.c Manaecmcnl Divi,ion SAlVIPLE Ai'ifALYSIS REQUEST S1.atc La.boralOry of Public Hu.Ith P.O. Box 28047, 306 N. Wilmington St. Ralciyh, North Cm:,.lina 27611-3047 lteNumber 11ameofSite '1teLoc.:ition Alt O (20 I (oQW ;) ,,:;-1) Sampl~ID Nu, ·co-003-SL 08/10/98 1310 GRAB . . . .·. 12345678 CD081098, HC D. WILSON Ori de x Dev m S , ·fe..---Collected By_ so IL . · ~ { . } 1 •!NORG-CLP· METALS · Soil ' 9 -a•--•-.-••-·---. {) X f:i}. C(,'J I\ 0 Date Collected lgency: Hazardous Waste Solid Waste _0uperfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) I Environmental Concentrate Comments arsenic -barium - Ground Water (I) Solid (5) cadmium ---I_ -chromium Surface Water (2) Liquid (6) lead -- -mercury --Soil (3) Sludge (7) selenium -- -silver Other (4) Other (8) --- I - - Organ.ic Chemistry Inorgan.ic Chemistry -. ~arameter Results (mg/I) ~eter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS anttmo~y L.. :;). -benzene = Acid:BiN Ext. _J,.,Asenic _8. -carbon tetrachloride ~ 24-D L _),,rtium __ ao -·-· chlordane -------· --· -,-, -·----·-·-· ---·-·-···-···---2,4,5-TP(S,Ivex) _ beryllium -chlorobenune chlordane .. --v"'1'1miurn .L... 10 chloroform - ~ heptachlor -chloride -o-cresol hexachlorobe::uene ~omium· \QD -m-cresol hexachlorobutadiene cobalt p-cresol fapper - endrin .l4 .cresol ~ - lindane fluoride 1,4-dichloroben.zene -- rnethoxychlor iron 1,2-<lichloroethane --toxaphene ~ad 1.,1:,, -1, 1-dichloroethylene ~ -manganese -2, 4-dichl a roe thy lene ~ercury ..,__o.oB -heptachlor ~eke! I a, hexachlorobenzene -nitrate hexachlorobutadiene - ~enium -,:__ di ~ hexachloroethane -~ver <.. }l\ -methyl ethyl ketone l . FOR LAB USE ONL y sulfates nitrobenzene --thallium penta.chloropbenol -- ate Received -vanadium pyridine -__k:""zinc \SD tetraChloroethylcne IDate Extracted - -pH -frichJorOethy Jene -conductivity -2, 4,5-trichlorophenol Date Analyzed -TDS 2,4 ,6-trichloropheno! - IRcported By -flash point -vinyl chloride --endrin lindane -- IDate Repeft'1142 AUG 17~6 --m_ethoxychlor --toxaphene Lab Number 2,4-D -- --2,4,5-TP (Silvex) DHS 3191 (R~vi5cd 11/93) I I 'NC Depl.rtmcnt of Environment, Health, & Natural Resource, Solid Wane Management Divi,ion SAMJ'LE ANALYSIS REQUEST St.ate LaboralOry of Public Health P.O. Box 28047, 306 N. Wilming-..on Sl. R.1.lci1:h, North C.1.rolin127611·8047 l~-~u-~b:r Aft ~)?_P / (oo_(p ;:},s-0 SampleID_Numbe, · COsl03-SL 08/10/98 1310 GRAB 12345678 C0081098, NC · 0. WILSON - . NameofSite ---Cr,-iteY, Do✓ «I S, ·fe.--:: Collected By SOIL I · ~ · !NORG-CLP teLocation {) X -1-o ry; ft} C'.-, Date Collected _0uperfund Hazardous Waste Solid Waste Sample Type I Environmental Concentr.ite Solid (5) I- Ground Water (I) Surface Water (2) Soil (3) Other (4) Liquid (6) Sludge (7) Other (8) Organic Chemistry arameter Results (mg/I) P&T:GC/MS Acid:B/N Ext. 2,4-D 2,4,5-TP(Silvex) chlordane heptachlor hexachlorobenzene _____ _ bexachlorobutadiene,_ ____ _ endrin lindane methoxychlor· tox.aphene FOR LAB USE ONLY Late Received _________ _ ~ate Extracted "oate Analyzed _________ _ teported By Date Re.J?,.orted . • u 1.1:[~c.-iJ,....,_ AmU~G ,._.l 7"H'9,_,.,B __ Lab Number IDHS 3191 (Rov;,od 11193) Commenl~ Inorganic Chemistry Par~eter Results(mg/l)(mg/kg) ....\<'.'.'.' antimony _ _c4=-cl~---- __j,_,,-"1'senic _..L..-'-c'+_,_ __ _ -~um _.,,2~0,_ __ _ beryllium ~mium --"'--~)o-__ _ chloride ~omium -~10,=,,0,__ __ _ _ c__g!,alt __0opper -~a=o~--- tluoride iron ~ad 5lo _ manganese ______ _ ~ercury ~ .0 -0 8 ~eke! ""-10 nitrate ~enium ~ver sulfates thallium _ vanadium ~c "---10 150 pH conductivity -------TDS flash point ______ _ KETALS Soil 12 ~----------~-~ TCLP Compounds Inorganic Compounds arsenic barium cadmium chromium lead mercury selenium silver Results(mg/1) Organic Compounds Results(mg/1) benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol p-cresol cresol 1,4-dichlorobenzene 1,2-dichloroethane l, 1-dichloroethylene ______ _ 2,4-dichloroetbylene ______ _ heptachlor hexachlorobenzene hexachlorobutadiene ~ bexachloroetbane methyl _ethyl ketone nitrobenzene pentachloropbenol pyridine tetraChloroethylene trichloroethylene 2,4,5-trichlorophenol ------- -------2,4,6-trichlorophenol vinyl chloride ------- endri.n lindane methoxychlor toxaphene 2,4-D 2,4,5-TP (Silvex) I ,NC Dep.inmcnt of Environment, Hc.alth, & Narun.1 Ruourccs Solid Wuu: Muugcmcnt Divi,ion SMIPLE AL'l'ALYSIS REQUEST St.ate Labon.1.0ry of Public Health P.O. Box 18047, 306 N. Wilmington St. Ralci:i:h, Nonh'C.arolina 27611-8047 tNum•ber Name of Site lteLoC3tion Alt O (J)O I (bo(p 2.<1J Sample ID Numb, CD-OOScSL 08/10/98 1245 GRAB . . • . . . 12345678 ·CD081098, NC D. WILSON Cridex f)a 1 m S ,·fe= Collecte<iBy_ SOIL. . ~ { ) 1 !NORG-CLP · HEJALS Soil -· -· ' 18 -· - {) )( tf2 C(') I\ 0 Date Collected ___ _ 'ency: Hazardous Waste Solid Waste _0uperfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) I Environmental Concentrate Comments -arsenic barium - Ground Water (1) Solid (5) cadmium ---chromium I-- Surface Water (2) Liquid (6) lead -- -mercury Soil (3) Sludge (7) selenium r --silver - Other (4) -Other (8) - -I - Organic Chemistry Inorganic Chemistry - tarneter Results (mg/I) ~eter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS antimony "'-,t, benzene - -Acid:B/N Ext. ~senic '4 carbon tetrachloride - I= 2,4-D b«tium ___ 40 ___ . --·. i;hlordane ------··,, _ _.,.beryllium ····-··--- 2,4,5-TP(Silvex) -chlorobenz.ene chlordane ~dmium ..t.. 10 chloroform -. - beptachlor chloride o-cresol F -- hexachlorobe:izene ~oIIUurn \;),Q rn-cresol - hexachlorobutadierie ~alt p-cresol . -- -. endrin per .al§ cresol -~ lindane fluoride 1,4-dichlorobenzene -- methoxychlor iron 1,2-dichloroethane -- -toxaphene ~ad Sa -1, 1-dichloroethylene I= -manganese 2, 4-dichloroethylene - ~ercury L.. a -£"I 8 -heptachlor -~eke! l 'J,, hexachlorobenzene -nitrate hexachlorobutadiene .I= ~en.ium -..,_ d-, ~ hexachloroelhaoe -~ver 4\o -methyl ethyl ketone FOR LAB USE ONLY sulfates nitrobenzene -- late Received -thallium pent.achloropbenol -vanadium pyridine - .k:""zinc 'i.80 -tetrachloroetbylene (ate Extracted -pH trichloroethylene - -conductivity -2 ,4,5-trichlorophenol ate Analyzed -TDS 2, 4,6-trichlorophenol - teported By -flash point -vinyl chloride endrin ~ -lindane --lie Repoo1_ti4~ AUG 1798 --methoxychlor toxaphene --b Number 2,4:D -- --2,4,5-TP (Silvex) r HS 3191 (Revised 11/93) I Ne Depa~mcnt of Enviionmcnt, Hc.alth, & Nawn.I Ruourccs Solid Wu~ M•n.aiemcnt Divi,ion SAMPLE Ai'IALYSIS REQUEST St.ate Laboratory of Public Hu!th P.O. Box 28047, 306 N. Wilmington St. Ralcii;h, Nonh C1.rolina 27611-8047 INumbcr [ eofSite Loc:ition Alt O (!)0 I (oo(p ;:2,<1J Sample!DNumber CD-006-SL 08/10/98 _1705_ GRAB -----·-12345678 C0081098, NC D. WILSON Crisfex Dc,1 m .S, ·fe-Collected By_-sorL _ /) j !NORG-CLP HETALS Soil Q 'i. t:fl_ r/, A} C,, Date Collected I ------···---21 ) 'ency: Haurdous W a.ste Solid Waste _0uperfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) t nvironmental Concentrate Comments arseruc -barium - Ground Water (I) Solid (5) cadmium --- l -chromium Surface Water (2) Liquid (6) -le:id --mercury t Soil (3) Sludge (7) selenium -- -silver Other (4) Other (8) --- i - - Organic Chemistry Inorganic Chemistry - trameter Results (mg/I) ~eter Results(mg/l)(mg/kg) Organic Com pounds Results(mg/1) _ P&T:GC/MS antimony L. I benzene - -Acid:B/N Ext. ---J..---"1'SC ru C 8 carbon tetrachloride - l 2.4-D ---·----------1 _J,atium ____ 1,c _________ ---chlordane ··;,.,::-,---·---· -----. 2,4,5-TP(Silvex) __ beryllium -chlorobenzene -chlordane . --1.----"'.f'd mi um _b]O chloroform - l hept.ichlor -chloride o-cresol - hexachloroben.zene ~oroj urn \Ol) m-cresol - hexachlorobut.adiene ~alt . p-cresol -- I= endrin per I':\ cresol - lindane fluoride 1,4-dichJorobenz.ene -- rnethoxychlor iron 1,2-<lichloroethane --- toxaphene ~ad IC I, 1-dichJoroethylene I-- . -manganese -2, 4-dichloroetbylene ~ercury .t.D.OB hept.ichJor - --~eke! L.. \t, -hexachlorobenzene t nitrate bexachlorobutadieoe ~eniurn -.l. d, ~ hexachloroethane - ~ver ..:.io -methyl ethyl ketone I FOR LAB USE ONL y -sulfates nitrobenzene thalli~rn - --pentacWoropbenol ate Received -vanadium pyridine - ~zinc ~l. -tetraC:hloroethylene •·ate E~tracted -pH trichloroethylene - -conductivity 2, 4, 5-trichJo rophenol -Date Analyzed -TDS 2,4,6-trichlorophenol - leported By -flash point . vinyl chloride - ---endrin lindane -- ('e Reported . · --met.hoxychlor 011145 AUG 1798 --toxaphene b Number 2,4-D -- --2,4,5-TP (Silvex) HS 3191 (Revi~ed 12/93) I ' I ' NC D~a.n:ment of Environment, H~lth, & Nawn.I Ruourcc, Solid Wu~ Management Divi,ion SAMPLE ANALYSIS REQUEST SLll.te L&borstory of Public Health P.O. Box 28047, 306 N. Wilmington St. R.dei1:h, North C1.ro!in1 27611·8047 lleNumber Alto (201 (oo(p ,1.C:1J SamplelDNumber. CD-007-SL 08/11/98 1900 GRAB 12345678 CD081098, NC o. WILSON C · ,,J-. h 5 ·f. SOIL Name of Sile Ire Location Cle)( VCV m ,'e..--: Collected By __ !NORG-CLP HETALS . Soil {) I.. 1-o C(,j fl) G DateCollected ___ ;::::::::=======----3:_:2:__ __ lgeocy: . __ Hazardous Wasle Solid Waste 0uperfund Sample Type -1 Environmental Concentrate Ground Water (I) Solid (5) I-Surface Water (2) Liquid (6) .-Soil (3) Sludge (7) Other ( 4) Other (8) Organic Chemistry arameter P&T:GC/MS Acid: BIN Ext. 2 ,4.n 2,4,5-TP(S;ivex) chlordane bepuichlor Results (mg/I) hexachloroben.zene _____ _ hexachlarobutadiene'-----'--- endri.n lindane methoxychlor toxapht:ne FOR LAB USE ONLY Late Received __________ _ r•te Extracted Date Analyzed _________ _ teported By Date R~Ojled · I u 111,_.4,__o-AU_G ....... 17=9~5 - Lib Number • ---------- IDHS 3191 (Revised \:2,'93) Commentli Inorganic Chemistry Par";]Jeler Results(mg/l)(mg/kg) _L antimony L... I d. -J,..-,-"1'Senic -"'--'--':\:.__ __ _ -j_,.),atium __ ..l.._~ ____ . _ beryllium -~mium _,,t._,Lo=---- chloride ~omium cobalt ~pper fluoride iron ~ead \0 _ manganese ______ _ ~ercury ~eke! nitrate ~enium ~ver sulfates thallium vanadium __k:""'zinc Yla pH conductivity -------TDS flash point ______ _ TCLP Compounds Inorganic Compounds arsenic barium cadmium chromium lead mercury selenium silver Organic Compounds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol p-cresol cresol 1,4-dichlorobenzeae 1,2-dichloioethane Results(mg/1) Results(mg/1) l, 1-dichloroethyle□e ______ _ 2,4-dichloroetbylene ______ _ beptachlor hexachlorobenzene bexachlorobutadieae ~ hexachloroetbane methyl ethyl ketone nitrobenzene pentacbloropbenol pyridine tetr3.Ch1oroethy lene trichloroethy lene ----- 2,4,5-trichlorophe□ol ______ _ 2,4,6-trichlorophenol ______ _ vinyl chloride endrin lindane methoxycblor toxaphene 2,4-D 2,4,5-TP (Silvcx) I ' NC Dcpanment. of Environment, Hu.Ith, & Nawn.I Re,,ources Solid Wut.e Management Divi,ion SMIPLE Ai'IAL YSIS REQUEST SL.ate Labon.LOry of Pubiic He.alth P.O. Box 28047, 306 N. Wilmington St. Ralci~h. North Carolina 27611-&047 l te Number _,/0'-'<->C--"1'-'0"-"{2<.IOLL/ --"(o.c,O"'-"'(p'-"'Ju,_,~_1)-'='--__ Sample ID Number/.-CD~.008-SL 08/11/98 1900 GRAB 12345678 CD081098, NC D. WILSON NameofSite Cci dex Do, in s ,·fe-Collected By_·_ SOIL !NORG-CLP HET ALS Soi I ltel.oc.:itio□ __,,Q"--Ax-1-h2.u...LC.c..0cLj--1/c...l/<.....>e,..,~::.._ ___ · Date Co!lected ____ -;::======---====3=5===--- 0uperfund TCLP Compounds Hazardous Waste Solid Waste Sample Type 1 Environmental Concentrate Solid (5) Ground Water (I) I-Surface Water (2) Liquid (6) · Soil (3) Sludge (7) L Other (4) Other (8) Organic Chemistry 11f ararnetcr I--P&T:GC/MS Acid: BIN Ext. 2."-D 2,4,5-TP(Siivex) chlordane heptacWor Results (mg/I) hexachloroben.zene _____ _ bexachlorobutadiene '------ endrin lindane methoxychlor toxaphene FOR LAB USE ONLY Jate Received _________ _ ~ate Extracted lloate Analyzed _________ _ reported By Date Rep°(j°fii4",'.' AUG 1"79B lub Number ID>IS 3191 (R,vised J'.'./93) Comments Inorganic Chemistry Par";)Jeter Results(mg/I)(mg/kg) ..!L antimony 4 \. do. -V"1"eruc -~b-___ _ _ -i,.-),atium ·--~-~,{),._,_ __ _ beryllium ~mium -=L..~~\Q..,_ __ _ chloride .~omiurn _ c..99alt __i.c'copper fluoride iron ~ead 110 IQ _ manganese ______ _ ~ercury ~eke! nitrate ~eniurn ~ver sulfates thallium vanadium .J.c"linc pH LlO conductivity ______ _ TDS flash point ______ _ Inorganic Compounds arsenic barium cadmium chromium lead mercury selenium silver Orgaruc Compounds benzene carbcn tetrachloride chlordane chJorobenzenl! chloroform o-cresol rn-cresol p~resol cresol 1,4-dichlorobenzene 1,2-<lichloroethane Results(mg/1) Results(mg/1) 1, 1-dichloroethylene ______ _ 2,4-dichloroetbylene ______ _ heptachlor hexachlorobenzene hexachlorobutadiene ______ _ .,. hexachloroetbane methyl ethyl ketone nitrobenzene pentachlorophenol pyridine tetraChloroethylene tricWoroethylene 2,4,5-trichlorophenol ______ _ 2,4,6-JrichJorophenol ______ _ vinyl chloride · endrin lindane methoxychlor toxaphene 2,4-D 2,4,5-TP (Silvex) I ' NC D~anmcnt of Enviionment, Hc.allh, & N1.wn.l Ruourcei; Solid Wane Management Divi,ion SMIPLE Ai"\'ALYSIS REQUEST St.ate Laboratory of Public Health P.O. Box 18047, 306 N. Wilmington St. Ralei~h, Nonh C.1.rolin1. 27611-8047 iameofSite -iteLoc:i.tion Aft O (20 I (oo(p ,1.<1J SamplelDNumi CD-009-SL 08/12/98 1450 GRAB /'/ _L _ _/ 12345678 CD081098, NC D. WILSON vci "iL(X Do✓ m .) , -T~ u:illectedBy _ SOIL _ /1 ~ { } , !NORG-CLP METALS Soil ' 38 -ty_ X t1} CC:'J /1. 0 Date Collected lgency: Hazardous Waste Solid Waste _0uperfund TCLP Compounds ---- Sample Type Inorganic Compowuls Results(mg/1) I Environmental Concentrate Comments -a.rseruc · barium - Ground Water(!) Solid (5) -cadmium -- L chromium Liquid (6) - Surface Water (2) lead -- -mercury .--Soil (3) Sludge (7) -selenium --silver Other (4) Other (8) --- I - - Organic Chemistry Inorganic Chemistry - farameter Results (mg/I) ~eter Results(mg/l)(mg/kg) Organic Com pounds Results(mg/1) P&T:GC/MS antimony £__ ). :l... benzene ..L i - Acid: BIN Ext. -J..,,-"1"S eru C -carbon tetrachloride E 7. •-D --h,.,-b<rrium __ ...2:,_D. ---chlordane -. ··-···" .. -.•···' ····-·-. 2,4,5-TP(Stlvex) _ beryllium -chJorobenzent: -chlordane . ~ mi urn L.. ,o -chloroform I= hepL1chlor -chloride -o-cresol hexachlorobenze:::ie ---J,..----"b:romiurn \lH) m-cresol - ___ hexachlorobutadiene ~rut p-cresol - 1: endrin per -~~ cresol - lindane -fluoride 1,4-dichlorobenzene - -methoxycWor -iron -1,2-<lichloroethane toxaphene ~ad \4 -I, 1-dichloroethylene I -manganese -2, 4-dich loroetby I ene ~ercury .L..O~oS -bepL1chlor -~eke! IQ hexachlorobenzene -1-nitrate hexachlorobutadiene ~enium -<.d,. ~ hexachloroethane - ~Iver 4-,o -methyl ethyl ketone I FOR LAB USE ONL y -sylfates -nitroben.zene -thallium pentachlorophenol - Date Received -vanadium pyridine - ~nc 5ll -tetrachloroeth y lene I Date Extr~cted --pH -trichJoroethylene -conductivity -2A,5-trichlorophenol Date Anruyzed -TDS 2, 4, 6-tri chl o rophenol -I Reported By -flash point -vinyl chloride -endrin -lindane -- Date Reported methoxychlor I 011148 AUG 1798 -- --toxaphene Lib Number 2,4-D -- --2,4,5-TP (Silvcx) DHS 3191 (Revi5ed 11/93) I I ' NC Depu'tmcnt of Environment, Haith,&. Nawral RC.f.ource, Solid Wute Management Divi,ion SMIPLE Ai','ALYSIS REQUEST Sl4te Laboratory of Public Hulth P.O. Box 28047, 306 N. Wilmington St. Ra!ciyh, North C.rolina 27611-8047 l ie Number _,/0'-"-.l,C-.::'-><0'-"'(2-'-'0'----'/'-{i"'o"'Q:..!J(p'--"2'-''-'<-V-=---Sample ID Numb, C0-014-SO. 08/12/98 .1015 . GRAB .. /1 · 12345678 CD081098, NC O. WILSON NameofSite L/ci dex Dcu m s ,-t~ Collected By_._ !NORG-CLP I . r, /) IA) ~' teLoc:ition--'1y"--x"-l-ro.£LLU-<.0A)--,l--'!J"---"-~""-----DateCollected _0uperfund -gency: __ Hazardous Waste Sample Type Environment.al Concentrate Solid Waste Comments KETALS Sedi1ent 50 TCLP Compounds Inorganic Compounds arsenic barium Results(mg/1) I Ground Water (I) Solid (5) _,?_ce:-=.jyou. -=/ ~"--'V"'-'Lm.,___C-<.Ji-d.__.::_·...:a:..:.//{~!&0'-'= ~ cadmium 1--Surface Water (2) Soil (3) L Other (4) Sludge (7) Other (8) Organic Chemistry ara;:rGC/MS _ Acid:B/N Ext. 2,4-D 2,4,5-TP(Silvex) chlordane heptacWor hexachlorobenzene Results (mg/I) ------bexachlorobutadienec.._ ____ _ endri.n lindane methoxycWor toxaphene Inorganic Chemistry Par';:9)eter Results(mg/l)(mg/kg) _L antimony c:..t..=.l'-'''--'d>""----- ~senic _<-=.4..,___ ___ _ _l _J,a:tium _'il:L. _________ _ _: beryllium -!.......-6dmium _.t...-=-cl,.,,0.,__ __ _ chloride ~omium _ __,)ul"-l"I.,_ __ _ _ cJ!,all __0opper ae fluoride iron ~ad _ manganese ______ _ ~ercury ~ckel 0. \c.:,;d\'-'--- J__ \l'ls,JL_ __ _ nitrate ~enium -----------~----1 ~Iver -<. \ 0 FOR LAB USE ONLY ~ate .Recei.ved _________ _ lDate Extracted ate Analyzed _________ _ reported By Date R;Ported · I ut.11~4:J~' A=□c-1~,=9s~- Lab Number IDHS 3191 (Rcvi,ed l:'193) sulfates thallium· vaniidium ~nc pH 350 conductivity ______ _ TDS flash point chromium lead mercury selenium silver Organic Compounds benzene carbon tetrachloride cWordane cWorobenzene chloroform o-cresol m-cresol p-cresol cresol 1,4-dichlorobenzene 1,2-dicWoroethane Results(mg/1) I, 1-dicWoroethylene ______ _ 2,4-dichloroetbyleoe ______ _ beptacWor hexachlorobenzene bexachlorobutadiene ... hexachloroethane methyl ethyl ketone nitrobenzene pentachloropbenol pyridine tetrachloroethylene _tricWoroetbylene ------- 2,4,5-lrichlorophenol ______ _ 2,4,6-tricWoroj,henol ______ _ vinyl cWoride endrin lindane melhoxychlor toxaphene 2,4-D 2,4,5-TP (Silvex) I ' NC Department of Environment, Health, & N.10Jral Ruourccs Solid Wut.e Man.&gcmcnt Divi,ion SMrPLE A.t~ALYSIS REQUEST SLatc LaboralOry of Public Health P.O. Box 28047, 306 N. Wilmington St. Ralcii;h, Nonh C.a.rolina 27611-8047 I 't/, Q (')0 / I 01 /'"J ..--,,ri S lclDNumb, C0-015-SO 08/12/98 1040 GRAB iteNumbcr_,/V'--"-'lv..::...,,<...J.,'-l.LL--"{O"-'"'-"'(ll'-,u;2iu·..L)_=-.V __ amp 12345678 CD081098, NC -D. WILSON Name of Site Cri de 'I, t>n✓ m s I ·t~ O,llectedBy_._ ·-INORG-CLP liteLoc,tion {) 'i. &. '"j f,j ~ . Date Collected Sediment 53 j fgency: Hazardous Waste Solid Waste _0uperfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) I Environmental Concentrate Comments -arsenic barium R,rfy ,/e. I/ ,v) - Ground Water (1) Sc!id (5) cadmium --' - U!/+teM. t'rvi..-fr i/Y/ chromium I-- Surface Water (2) Liquid (6) -lead - Su517e tfe/ -mercury Soil (3) Sludge (7) -selenium -I L silver - Other (4) Other (8) --- I - Organic Chemistry Inorganic Chemistry - tameter · Results (mg/I) ~eter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS . ... · ai1timony ~d, benzene 4-~ - _ Ac,d:E/N Ext. -v-"1se.nic -carbon tetrachloride I= 7,4-D ~um --~0 .... ---·-·· ---chlordane -·---------···-----·------· 2,4,5-TP(Silvex) _ berylliura -chlorobenz.ene chlordane ~dmium L...)0 -chloroform _ heptachlor -chloride o-cresol --~ hexachlorobenz.ene ~omium no -m-cresol _ hexachlcrobut.aUiene ~alt -p-cresol -endri.n per __5lq cresol - I lindane fh.ioride 1,4-dichlorobenz.ene -- methoxychlor -iron 1,2-dichloroethane - -toxaphene ~ad :l.l"\ -I, 1-dichloroethylene I= -manganese -2, 4-d ichloroeth y I ene ~ere u ry 0~3la -heptachlor Yn'fckel 410 hexachl0robenzene --nitrate hexachlorobutadiene 11-. ~eniurn -...,__ 4\ -~ hexachloroelhane - ~ver L.. ,o methyl ethyl ketone ·- FOR LAB USE ONLY -. sulfates nitrobenzene - lnate Received -thallium pentachlorophenol -vanadium pyridine - ~nc '-t 2.0 -tetrachloroeth y lene 1 Date Extracted -pH -trichloroethylene -conductivity -2,4,5-trichlorophenol Date Analyzed -TDS 2,4 ,6-trichlorophenol - -Dash point -vinyl chloride I Reported By --endrin lindane -- Date Reported --methoxycblor I 01-1150 AUG 1198 --· toxaphene L:tb Number 2,4-D -- --2,4,5-TP (Silvex) I DHS 3i91 (Revised 11193) . I ' NC Dep11rtment of Environment, Hulth, &. Nan.ir:al Ruources Solid WuLc Muugcmcm Divi,ion SAlvrPLE At'!ALYSIS REQUEST St.ace Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Ralei1,:h, North C.1rolin1 27611-8047 l te Number Alt O (!)0 J (oo(p :) , <-V Sample ID Number/ CD-016-SD 08/12/98 1200 GRAB --------. 12345678 CD081098;· NC D: WILSON NameofSite Cridex Dcu 01 s ,·te.--: Collected By_· --!NORG-CLP· HETALS Sedi1ent I teLoc:ition -CQ<-.Ax+-&2-"'-'c'--'-';,-;L~-·· _· -1/t-"/'-'-e,""1 '--___ Date Collected ____ --;:::::===========-=-==:=====5=6====-, . lgency: __ Hazardous Waste Solid Waste 0uperfund TCLP Compounds Sample Type I Environ.;nental Concentr.ite Ground Water (1) Solid (5) •-Surface Water (2) Liquid (6) .-Soil (3) Sludge (7) OlLer (4) Other (8) I Organic Chemistry arameter Results (mg/I) P&T:GC/MS Acid:B/N Ext. o t..n .. , --..• - 2,4,5-TP(Silvex) chlordane heptachlor hexachlorobe22ene -~----hex:i.chlorobut.1<liene,:._ ____ _ endrin lind:me methoxychlor toxaphene FOR LAB USE ONLY · IDate R~eived ----------1 Date Extracted _________ ~ Date Analyzed _________ _ .Reported By Date R~ortfd I u 11r-stt-tActtf'LJF,"-+'l7"1-99~B - Lab Number IDHS 3191 (Revised l'.2/93) Comments p r;:-f-ro /.e v' 111 iAfvt-+4-M,/-1.t'.,h ~ .5..Jsp ~ c,1'.e_ £. Inorganic Chemistry Par~eter Results(mg/l)(mg/kg) _L antimony _,_I.,_.~~"----- _j,.,--"fsenic _~...c...J,\-..,_ ___ _ _ ¾,.,,b,rtium . _ '::\l:L ____ ..... _ beryllium. ______ _ ~mium _..l...__c,_..,)l),.,_ __ _ chloride ~omiurn _:_ "39 al t __jC'copper fluoride iron ~ad 110 10 _ manganese ______ _ ~ercury ~eke! nitrate 0e1eniurn ~ver sulfates thallium vanadium ~zinc pH .t.... \0 conductivity ______ _ TDS flash point ______ _ Inorganic Compounds Results(mg/1) arsenic barium cadmium chromium lead mercury selenium silver Organic Compounds Results(mg/1) benzene carbon tetrachloride ______ _ chlordane chlorobenzene chloroform o-cresol m-cresol p-cresol cresol 1,4-dichlorobenzene -------1,2-dichloroethane I, 1-dichloroethylene ______ _ 2,4-dichloroethylene ______ _ beptachlor hexachlorobenzene hexachlorobutadiene --~---- .,. hexachloroethane methyl ethyl ketone nitrobenzene pentachloropbenol pyridine tetraC:hloroethylene trichloroethylene 2,4,5-trichlorophenol ______ _ 2,4,6-trichlorophenol ______ _ vinyl chloride endrin lindane meth.oxychlor toxaphent! 2,4-D 2,4,5-TP (Silvex) I ' NC Dci>artmcnt of Environment, SMIPLE Ai~ALYSIS REQUEST St.ate La.boratory of Public Health P.O. Box 28047, 306 N. Wilmington St. · Huhh, &. Narural RC1ourccs Solid Wuu: Man.agcment Divi,ion Raleigh, North Cuolina 27611-8047 lite Number /i.lt O (20 I (oQw J .<V Sample!DNumb, CD-017-SL 08/12/98 1140 GRAB 12345678 C0081098, NC D. WILSON SOIL Name of Site liteLoc;ition Crisfex Do✓ m ,5 1 ·fe-Collected By_ !NORG-CLP HE! ALS Soil {)x&J_r,;j tJ~ i lgency: Hazardous Waste Solid Waste _0uperfund TCLP Compounds ---- Date Collected 59 Sample Type Inorganic· Compounds Results(mg/1) I Environmental Concentrate Comments -arsenic -barium Ground Water (1) Solid (5) cadmium --- L -chromium Surface Water (2) Liquid (6) -le.id --mercury .-Soil (3) Sludge (7) . selenium --silver - -Other ( 4) -Other (8) - -t - Organic Chemistry Inorganic Chemistry - rarameter Results (mg/I) ~eter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) _ P&T:GC/MS anlimony .,__ '-J._ -benzene Acid: BIN Ext. -v-"1'senic ..:.. lj--carbon tetrachloride ,- II= 1,4-D -_ /,_,)>irti um _._,oo .. --chlordane -·-·-···--··-·------·· 2,4,5-TP(Silvex) _ beryllium -chloroben.zene -chlordane ~mium ,t__\O chloroform - II= beptachlor -chloride -o-cresol hexachloroben.zene ~omium , ,1.. oo m-cresol - hex:ichlorobutadiene cobalt p-cresol -0pper - -endrin 3';6 cresol I - -iindane -fluoride 1,4-dichloroben.zene - -methoxychlor iron 1,2-<lichloroethane -~9 - -toxaphene ~ad -l, 1-dichloroethylene I --manganese -2, 4-d i chloroetby I ene -~ercury 0, ';b heptachlor - -~ckel \A -hexachlorobenzene I -nitrate hexachlorobutadiene ~eniurn -..-:..~ ~ hexachloroethane -·~ver -<10 -methyl ethyl ketone FOR LAB USE ONLY -sulfates nitrobenzene I Date Received - -thallium pentachlorophenol -vanadium pyridine /Bfo -__k""zinc -tetrachloroethylene I Date Ext~acted -pH trichloroethylene - -conductivity--2, 4,5-trichlorophenol Date Analyzed -TDS 2, 4, 6-trichlorophenol -I Reported By -0a.sh PC?int -vinyl chloride --endrin lindane -- Date Ro11J methoxychlor I · 152 AUG 1796 -- --toxaphene Lab Number · . 2,4-D -- --2,4,5-TP (Silvex) I DHS 3191 (Revised 1:2/93) ' I ' NC Dc!p1rtment of Environment, H,:.,.lth, & Nawn.I Ruourceli Solid Wutc Muugcment Division SMIPLE A.L'IAL YSIS REQUEST St.ate Laboratory of Public He1l!h P.O. Box 28047, 306 N. Wilmington St. Raleii;h, North c;.1.ro!ina 27611-8047 lite N:mbcr _,M~c,<;':_.!D~C2.!!0S<!..ll..cuU<o'.l<QCJ.U>eO...!(i2!..,._, ',_,_..--;_v'='---Sample rn Number/ NameofSite Cci dex Dn✓ m .s, ·fe-CollectedBy_· - litcLocation /) Y.. fr}_ re,j tJ G Date Collected C0-021-SL 08/13/98 1500 GRAB 12345678 CD081098, NC D. WILSON SOIL !NORG-CLP . METALS Soil 66 I .. lgency: Hazardous Waste Solid Waste _0uperfund TCLP Compounds ---- Sample Type Inorganic CompoWJds Results(mg/1) I Environmental Concentrate Comments -arsenic -barium Ground Water (1) Solid (5) -cadmium -- I--chromium Surface Water (2) Liquid (6) -lead - -mercury Soil (3) Sludge (7) -selenium .--silver - -Other (4) -Other (8) -I - Organic Chemistry Inorganic Chemistry - rarameter Results (mg/I) ~eter Results(mg/l)(mg/kg) Organic CompoWJds Results(mg/1) _ P&T:GC/MS anlnnony 4-Li -benzene -Acid: BIN Ext. ~senic .£... i\ carbon tetrachloride - I 2,4-D ----·-··------J J:,,rtium ---~-o ________ ·-chlordane .. ...,.,. ----·-·-·-· 2,4,5-TP(Silvex) _ beryllium -chlorobenzene chlordane ~dmium -"--10 chloroform -. - I heptachlor -chloride -o•cresol hexachlorobenzene · -1,..--"lrromi urn I IQ m-cresol - hexachlorobutadiene ~alt p-uesol -- endrin per J.. ID cresol -I lindane fluoride 1,4-dichlorobenzene -- I methoxychlor iron I, 2-dichloroethane --- -toxaph!!ne ~ad ~10 -1, 1-dichloroethylene II= -manganese -2, 4-dichloroethylene ~ercury L.o .a /ii -heptachlor -~ckel ..::. 10 hexach.lorobenzene - 11-- nitrate hexachlorobutadiene ~enium -L. ;;>-. ~ hexachloroethane - ~ver L..ta methyl ethyl ketone - FOR LAB USE ONLY -sulfates nitrobenz.ene I Date Received - -thallium pentachlorophenol -vanadium . pyridine - .JC"'zinc Zif -tetraC:hloroethylene I Date Extracted -pH -trichJoroethylene -conductiviry -2,4,5-trichlorophenol Date Analyzed -TDS 2, 4,6-trichlorophenol -I Reported By -flash point -vinyl chloride --endrin lindane -- Date R(}orted methoxychlor_ I tti53 AUG 1798 -- --toxaphene Lab Number 2,4-D -- --2,4,5-TP (Silvex) I DHS 3191 (Rtviml 11./93) I ' NC Dl:partmcnt of Environment, Health, & Nawral Rei.ources, Solid Wut.e M1n.1gemcnt Divi,ion SAMPLE Ai~ALYSIS REQUEST St.ate LaboraLOry of Public Health P .0. Box 28047, 306 N. Wilmington St. Ralci~h. North Carolina 27611-8047 ,,teNu'."bcr Alt D (20 I (oQw J <V Sample ID Number CD-022-SL 08/11/98 1340 GRAB ·-12345678 · CD081098, NC O. WILSON Name of Site lite Location Cri de)( Do✓ m s I ·te--Collected By SOIL j --!NORG-CLP METALS Soil {) Y, 1-o C<j jl/ Cc DateCollected ___ -;:::~----'---_.:_~6 9 lgency: Ha=dous Waste Solid Waste _0uperfund Sample Type I Environmental Concentrate Ground Water(!) Solid (5) L Surface Water (2) Liquid (6) .-Soil (3) Sludge (7) Other (4) Other (8) Organic Chemistry ar:uneter P&T:GC/MS Acid:B/N Ext. '.J,,d-"('. 2,4,5-TP(Silvex) chlordane heptachlor . hexaChlorobenzene Results (mg/I) ------hexachlorobutadiene =------ endri.n linc!J.ne methoxychlor toxaphene FOR LAB USE ONLY Late Received _________ _ .Date Extracted _________ _ Date Analyzed _________ _ .Reported By Date Repori,.d~ . I u i ..... __ !'""'1-5-;:,,-A-□-c ~1-7 9-5- Lab Number __ · _______ _ IDHS 319! (Revi:;cd 1:2/93) Comments Inorganic Chemistry Par":!)Jeler Results(mg/l)(mg/kg) _...y: antimony _,!..~\~, J.,=---- -V"1seruc _L..._~""~---- -.J_....J,,rri11m __ <t,..o_. ___ _ _ beryllium ~dmiuco _.,.L.=1,.,Q...,._ __ _ chloride ~omi urn 130 cobalt ~pper a4 fluoride iron ~ad :l.O -manganese ~er_cury ..:.o .¢6' ~eke! ,30 nitrate ~~nium .L. ~ ~Iver .L.. LO sulfates thallium vanadium ..Jc""zinc laid pH conductivity TDS flash point TCLP Compounds Inorganic Compounds arsenic barium cadmium chromium lead mercury selenium silver Results(mg/1) Organic Compounds Results(mg/1) benzene carbon tetrachloride chlordane chJorobenzene chloroform o-cresol m-cresol p-cresol cresol 1,4-dichloroben.zene 1,2-<lichloroethane 1,.1-dichloroethylene ______ _ 2, 4-dichloroetbylene heptachlor bexachlorobenzene hexachlorobutadieoe .,._ hexachloroethane methyl ethyl ketone nitrobenzene penlachlorophenol pyridine tetrachloroeth y Jene trichloroethylene 2,4,5-trichlorophenol 2,4, 6-trichlorophenol vinyl chloride endrin lindane methoxychlor toX.aphene 2,4-D 2,4,5-TP (Silvcx) ------- ------- ------- ------- I ' N<; Dq;i1r1ment of Environment, Hullh, &. Nawn.I Ruourccs Solid Wutc Management Divi,ion SA1V1PLE A.i'l"ALYSIS REQUEST State Laborat.ory of Public Health P.O. Box 28047, 306 N. Wilmington St. .i.teNumber..JM~ce::.'~o~o.LolL!./..J.{o<Llo.<.Ju"'-o...L2zu...,sJ,__,,1)<.__SamplclDNum· NameofSite Cridex Dev m s, ·fe-Collected By_; Raleii;h, North C1.ro!in1 27611-8047 C0-023-SL 08/11/98 1410 GRAB 12345678 C0081098, NC D. WILSON SOIL !NORG-CLP HETALS Soil I fl /) J AJ c~ itel.oc:ition _i;l';-l,c_.'x"-l-t1}_u_1-C...£(.,ij4---,,µf 1.,_ _ _,_~,e:_ ____ DateCollected _____ ;:=====--:------7:_:2:_ ___ _:..., _0u perfun d TCLP Compounds rgency:. __ Hazardous Waste · Sample Type Environment.al Concentrate I Ground Water {I) Solid (5) I-Surf.cc Water (2) Liquid (6) Solid Waste Comments Soil (3) Sludge (7) L I= Other (4) Other (8) Organic Chemistry P&T:GC/MS Acid: BIN Ext. ?,.A-D 2,4,5-TP(Silvex) chlordane bepL'lchlor hexachlorobenzene Results (mg/I) -------hexachlorobutadienec__ ____ _ endrin lindane methoxychlor t9xaphene Inorganic Chemistry Par~eter Results(mg/l)(mg/kg) _y: antimony 4'!.. \ • ';I. ~senic _L._i~---- -/;,-J,,rtium _LQD_ __ _ _ beryllium ~mium _c.L.=..,_,ll)...__ __ _ chloride ~omium _ "9'ait __0opper fluoride iron ~ad H ... _ manganese ______ _ ~ercury ~eke! nitrate ~eniurn ;----~----------, ~ver L. }Q FOR LAB USE ONLY loate Received_· _________ _ .Date ·Extracted Date Analyzed _________ _ IR.eported By Date Repo9,eq I · u 1 ..... 11....,~-);:-;---Au--c ..... 1-i 9~5---- Lab Number IDHS lt91 (Rcvi,ed 12/93) sulfates thallium vanadium _JC'."zinc pH conductivity ______ _ TDS flash point ______ _ Inorganic Compounds arsenic barium cadmium chromium lead mercury selenium silver Organic Compounds benzene carbon tetra.chloride chlordane chlorobenzene chloroform o-cresol m-cresol p-cresol cresol 1,4-dichlorobenzene 1,2-dichloroethane Results(mg/1) Results(mg/1) 1, 1-dichJoroethylene -------2,4-dichloroethylene ______ _ bepL'lchlor bexachlorobenzene hexachlorobutadiene .,._ hexachloroethane. methyl ethyl ketone nitrobenzene penL'lchlorophenol pyridine tetrachloroe~hylene trichJoroethylene 2,4,5-trichJorophenol 2,4,6-trichlorophenol vinyl chloride endrin lindane methoxychlor toxaphene 2,4-D 2,4,5-TP (Silvex) ------- ------- ------- I ' NC Dq)an.ment of Environment, Huhh, & Natural R«ources Solid Wane Management Divi,ion SMIPLE Ai'l'AL YSIS REQUEST St.ate U.boi:aLOry of Public Hu.Ith P.O. Box 28047, 306 N. Wilmington St. Ralcii,:h, North Carolina 27611-8047 lu:Number !It O (')Q/ (oo(p 2.<1J C0-024-SO 081 Sample ID Numbe. 12345678 10198 1628 GRAB CD081098, NC D. WILSON NameofSite Orisfex. Do, 01 S 1 ·fe.---Collecte<lBy_· !NORG-CLP . . N£T ALS Sediment I . ri /) I A) ~~ teLocation -"l:,l"'---)(>+f12.u..LU-t.(A)-,.--,f'-"-l _ _,,.~=----Dau: Collected ____ ~==----- _0uperfund 75 TCLP Compounds l 1.gcncy: Ha=dous Waste Solid Waste · Sample Type I Environmental Concentrate Ground Water(!) Solid (5) L Surface Water (2) Liquid (6) .-Soil (3) Sludge (7) Other (4) Other (8) Organic Chemistry l arameter _ P&T:GC/MS Acid:B/N Ext. 2,•-D 2,4,5-TP(Silvex) chlordane hept.!chlor Results (mg/I) hexachlorobenzene _____ _ hexachlorobutadiene'------- endrin lindane · methoxychlor toxaphene l FOR LAB USE ONLY ate Received --'---------rate Extracted _________ _ Date Analyzed ________ ..c.._ .eported By Date Reported . l 01.1155 AUG 1798 ~ b Number I\ IDHS 3191 (Rov;scd 11/93) Comments Inorganic Chemistry Par";!Jleler Results(mg/l)(mg/kg) _y antimony ..L.. I . Ji -J...--"1'Senic __ .<._>,J,_ __ _ --1.,,-,Pllfium _;,.,.,o ___ _ _ beryllium ~mi um J... 1 0 chloride ~oqii urn -"_3],alt _0opper fluoride iron ~ad l 10 _ manganese----=-- ~ercury "'-o k o, 8 yfuckel L.. lC nitrate ~eniurn ~ver sulfates thallium vanadium ....lC'Zinc pH L.)Q ,3/a conductivity ______ _ TDS flash point Inorganic Com pounds arseruc barium cadmium chromium lead mercury selenium silver Organic Compounds benzene carbon te:rachloricle chJordanr:. chlorobellL!ne chloroform o-cresol rn-cresol p-cresol cresol 1,4-dichlorobenzene 1,2-dichloroethane Results(mg/1) Results(mg/1) I, 1-dichloroethylene -------2, 4-di ch loroethy I ene bept.!chlor hexachlorobenzene bexachlorobutadiene ... hexachloroethane methyl ethyl ketone nitrobenzene pentachlorophenol pyridine tetrar.hloroeth ylec.e trichloroethylene 2, 4, 5-tric hlorophenol 2,4 ,6-trichlorophenol vinyl chloride endrin lindane methoxychlor_ toXaphene 2,4-D 2,4,5-TP (Silvex) ------- ------- ------- ------- I ' NC DCl)artmcnt of Environment, Hc.allh, &:. Nan:ra.J Ruources Solid Wut.c Man.agcmcnt Division SMIPLE Ai'IALYSIS REQUEST St.ate L&boratory of Public Hc.alth P.O. Box 28047, 306 N. Wilmington St. Raleii;h, North Carolina 27611-8047 lite Number _,A!i-"--"~"'-'=0'-(2"'-"'0'---'l_(o""""o.,.w'--"'2'--''J.<_YJ=---Sample rn Numb NamcofSite Cr, dex Do, m 6, ·fe-Collected By_ C0-025-SO 08 12345678 C008i~~~98NC1620 GRAB • D, WILSON litel.oc.'.ltion /) x -bJ.. ,/'} Date Collected !NORG-CLP HETALS Sedi1ent ) , 82 ·- lgency: Ha=dous Waste Solid Waste _0uperfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) I Environmental Concentrate Comments arseruc -barium - Ground Water (!) Solid (5) -cadmium --- L -chromium Surface Water (2) Liquid (6) -le:id --mercury .-Soil (3) Sludge (7) selenium --silver - -Other (4) -Other (8) - -f - Organic Chemistry Inorganic Chemistry - rarameter Results (mg/I) ~eter Results(mg/1) (mg/kg) Orpnic Compounds Results(mg/1) __ P&T:GC/MS antimony .L. I. d:, bc~ne - -Acid:B/N Ext. --L.,--"1'S eni C -<... ':t carbon tetrachloride - I= 2,4-T) . -~um .L.U) ·-· chlordane ----------· .... ,_ ·---·-··· ·········--·-· 2,4,5-TP(Silvex) _ beryllium -ch!orobenzene chlordane ~d mi um ,t_ IQ chloroform -. - J= heptachlor chloride o-cresol -- hexachloroben.zene ....i---"lrro mi um 5B rn-cresol - hexachlorobut.adiene ~alt p-<:resol -- endrin per L..lo cresol I -lindane fluoride 1,4-dichlorobenzene --methoxychlor iron, 1,2-dichloroethane -- toxaphene ~ad 10 -I, 1-dichloroethylene I -manganese 2, 4-dichloroetbylenc -~ercury -L.0-08 -heptachlor -yfiickel .C..]0 hexachlorobenzene -t-nitrate hexachlorobutadiene ~en.ium ,L_d, - ~ hexachloroethane - ~Iver -L.. lo -methyl ethyl ketone FOR LAB USE ONLY sulfates nitroben.z.ene IDate Received ---thallium pe~tachloropbenol -- -vanadium pyridine -~nc 4;), tefraChlorOethylene - .Date Extracted -pH -trichloroethy Jene -conductivity -2 ,4,5-trichlorophenol Date Analyzed -TDS 2,4, 6-trichlorophenol - I Reported By -flash point -vinyl chloride --endri.n lindane -- .Date Repcffii58 AUC 1798 --methoxychlor toxaphc;ie -- Lab Number 2,4-D -- -2,4,5-TP (Silvcx) DHS 3191 (Revised 1::2/93) -I I 'NC DCl)anmcnt of Environment, Hc.allh, &. Nawral Ruources Solid WuLe Marugcmcnt Divi,ion SAJ'vIPLE Ai'l'ALYSIS REQUEST State LaboralOry of Public Hcah.h P.O. Box 28047, 306 N. Wilmington St. R1.lei1:h, North C1.ro!in• 27611·8047 lteNumber Alt O (20 I (oow J.<V Sample ID Numb, C0-026-SO 08/10/98 1650 GRAB 12345678 CD081098, NC D. WILSON NarncofSite Cri dex Do, Q1 s, ·fe__.... Collected By_· I !NORG-CLP HETALS Sediaent teLocation_,;(},c_t.Xy-bw:t...LU..1.'✓-"~-r--+fv-"-/-'-k""~::_ ___ DateCol!ecled ____ ----;::::======--.:..::==8=9====- Hazardous Waste Solid Waste _0uperfund Sample Type II En_vironment..'11 Concentrate Ground Water(!) Solid (5) II-Surface Water (2) Liquid (6) Ir Soil (3) Sludge (7) Other (4) Other (8) Organic Chemistry ltameter P&T:GC/MS Acid:B/N Ext. 2,4-D 2,4,5-TP(Siivex) chlordane beptachlor hexachloroben.z.ene Results (mg/I) ------bexachloro bu tadiene ~----- endrin lindane methoxychlor toxaphene FOR LAB USE ONLY Lale Received _________ _ rate Extracted _________ _ Date Analyzed _________ _ teported By • Date R(fffi-F-f'S§,,__.A-HPLJG-4-'17'+99-&-8 - Lab Number IDHS 3191 (Revised \2/93) Comments Inorganic Chemistry Par~eter Results(mg/l)(mg/kg) _L anltmony ~"'-==-.1.I _,.._,,t,,,_ __ _ s --J.,--"l'Seni C ~ um _ beryllium ~mium chloride ~omium _ "3'all __0opper f111oride iron ~ad z,o <Jo _ manganese ______ _ ~ercury ~eke! nitrate ~eniurn ~Iver slllfates thallium vanadium ~zin C pH <ID conductivity ______ _ TDS t:}ash p':)int ______ _ TCLP Compounds Inorganic Compounds arsenic barium cadmium chromium lead mercury selenium silver Results(mg/1) Organic Compounds Results(mg/1) benzene carbon tetrachloride chlordane ch1orobenz.ene chloroform o-cresol m-cresol p-cresol cresol 1,4-dichlorobenzene 1,2-dichloroethane l, 1-dichloroethylene ______ _ 2,4-dichloroetbyleoe ______ _ heptachlor bexachloroben.zene hexachlorobutadieoe ______ _ ... hexachloroethane methyl ethyl ketone nitrobenzene pentachlorophenol pyridine tetraChloroethy!ene trichloroethylene 2,4,5-trichloropheool ______ _ 2,4,6-trichlorophenol ______ _ vinyl chloride endrin lindane methoxychlor toxaphene 2,4-D 2,4,5-TP (Silvex) I NC Dep~rtmcnt of Environment, SAMPLE ANALYSIS REQUEST SL&tc LabonlOry of Public Hc.alth P.O. Box 18047, 306 N. Wilmington St. Solid ~uLe Muugement Divi,ion Raleii;h, Nonh Carolin• 27611-&047 .: l:<u".'~:r _4{4 p __ qgt_(~B0 2 ,r,q_ . Sa,nple ID Num~c C0-126-SO . 08/10/98 1650 GRAB ._:. c-: ,· i· ,: ·,+ficj'_ ,, ~:J .... •· .:.,:-~ 12345678 C0081098, NC 0. WILSON NamcofSite rt -5"Let,·•· ,µ£1✓ m o I Ter-: CollectedBy_·_ leLoc:ition () )( -1-o c~ .. /JG Date Collected !NORG-CLP KETALS Sedi1ent --·· .. . .ency: --Hazardou.s Wa.,te --Solid Waste _0uperfund TCLP Compounds 96 Sample Type Inorganic Compounds Results(mg/1) f "_vironmental Concentr.ite Comments arseruc -barium - Ground Water(!) Solid (5) -cadmium -- l chromium - Surface Water (2) Liquid (6) -lead --mercury t Soil (3) Sludge (7) -selenium -silver - -Other (4) -Other (8) - -rt -Organic Chemistry Inorganic Chemistry - tameter Results (mg/I) ~eter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) _ P&T:GC/MS antimony L, \. .;;I, -benzene -Acid: BIN Ext. --1.---"'1s eni c __ )1~ carbon tetrachloride - l 2,4-D -!,,),,,ti um ---chlordane -----·------·-- 2,4,5-TP(Silvex) _ beryllium -chlorobenzene -chlordane . ~mium <9.s chloroform - I= heptachlor -chloride -o-cresol hexachloroben.zene ~omiurn I l4 m-cresol - hexachlorobutadiene ~alt p-cresol -/3.1 - endrin per cresol r - lindane fluoride 1,4-dichlorobenzene -- rnethoxychlor· iron 1,2-<lichloroethane --<-9.6 - toxaphene ~ad -l, 1-dichloroethylene I= _ manganese -2,4-dich!oroetby lene ~ercu~ L..o-o.A -beptachlor -eke! 11.e, hexachlorobeo..zene - I= nitrate hexachlorobutadiene ~en.ium - L. d-. ~ hexachloroethane -~ver <9.B -methyl ethyl ketone I FOR LAB USE ONL y sulfates nitrobenzene -- -thallium pentachlorophenol - ate Received vanadium pyridine -~zinc 5.3 -tetraChloroethylene late Extracted -pH tricWoroethylene --conductivity -2,4,5-trichlorophenol Date Analyzed TDS 2,4,6-trichlorophenol -- leported By -flash point -vinyl chloride ··--endrin -lindane -- (te Reported --methoxychlor 01i1G0 AUG 1798 --toxaphene b Number 2,4-D -- --2,4,5-TP (Silvex) HS 3191 (Revised 12/93) I I , NC· De?artment of Environment, Health, &. N.awral Ruources Solid Wane M•n.a&-emem Divi,ion SAivIPLE Ai'IALYSIS REQUEST SL&.te Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Raleigh, North Carolina 27611-8047 lite Number _M'-"-'c.""':..:0><-'(2""-""D'-'l-"'(oC>o'--'(i""-o'-'2""-'-. '>.L.-::_1)=---Sample rn Number NameofSitc Cri d-ex Dev m s ,-fe--O:,llectedBy_·_ CD-018-SL ·08/13/98 1405 -GRAB 12345678 CD081098, HC D. WILSON SOIL !NORG-CLP I II /) I ~J ~~ iteLootion _,_/:,/,c__'xa.+f12_,_,__,_C,_,_/.,,;)Lc-~,'-'' l~ _ _,,_~=-----Date Collected _0uperfund Hazardous Waste Solid Waste Sample Type I Environmental Concentrate Ground Water (1) Solid (5) I-Surface Water (2) Soil (3) Other (4) Liquid (6) Sludge (7) Other (8) Organic Chemistry P&T:GC/MS Acid: BIN Ext. 2,4-D 2,4,5-TP(Silvex) chlordane heptachlor hexachlorobenzene Results (mg/I) ------hexachlorobutadiene ::._ ____ _ endrin lindane methoxychlor toxaphene FOR LAB USE ONLY IDate Received _________ _ .Date Extracted Date Analyzed _________ _ .Reported By .. _________ _ Date Reported . " I Otilt::if AUG 1 l 98 Lab Number IDHS 3l9l (Ra,i,cd 11193) Comments Inorganic Chemistry Par~eter Results(mg/l)(mg/kg) _y antnnony L.. \. ;,-, ~senic _<::s4'-!.----- -i,),<rtium _!cJD. ______ _ _ beryllium ~dmium chloride ~o mi um -:99alt ~opper fluoride iron ~ad <ID 7B /lo <JO _ manganese --~---- ~ercury ~eke! nitrate ~enium ~Iver sulfates thallium vanadium ~nc pH <to <10 flf, conductivity ______ _ TDS flash point KETALS Soil 118 TCLP Compounds Inorganic Compounds arse!llc barium cadmium chromium le:id mercury selenium silver Results(mg/1) Organic Compounds Rcsults(mg/1) benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol p-cresol cresoI ------- 1,4-dichlorobenzene ______ _ 1,2-dichloroethane I, 1-dichloroethylene ______ _ 2,4-dichloroelhylene · ______ _ heptachlor hexachlorobenzene hexachlorobutadiene ... hexachloroethane methyl ethyl ketone nitrobenz.ene pentacbloropbenol pyridine tetraChloroethylene tric~oroethylene ------- 2,4,5-trichlorophenol ______ _ 2,4,6-trichlorophenol ______ _ vinyl chloride endrin lindane methoxychlor toxapheno 2,4-D 2,4,5-TP (Silvex) I 'NC Dcp1artmcnt of Environment, SAIVIPLE Ai'7ALYSIS REQUEST SlAte L&bor1.tory of Public Hulth P.O. Box 18047, 306 N. Wilmington St. · He.alt.h, &. N1run.l Ruourcc, Solid WuLe Man.a.-cment Divi,ion Ra!eii:h, North Carolina 27611-8047 lteNumber Name of Site lteLoCJtion A/C, 0 (20 / (oQ(v ,~.C:-1) Sample!DNumber. CD-019-SL 08/13/98 1335 GRAB · 12345678 (0081098, NC D. WILSON Cri #ex Dev m · S, ·fe__... Collected By_·_ sorL ~ { } 1 !NORG-CLP KETALS Soil t) I,, ttJ_ C(,') /t_ 0 Date Collected 125 , tency: --Hazardoll5 Waste --Solid Waste _0uperfund TCLP Compounds Sample Type Inorganic Compounds Results(mg/1) I Environmental Concentraie Comments arseruc -barium . -- Ground Water (I) Solid (5) -cadmium -- L -chromium Surface Water (2) Liquid (6) -lead --mercury Soil (3) Sludge (7) selenium r --silver - -Other (4) -Other (8) - -I -Organic Chemistry Inorganic Chemistry - l:ameter Results (mg/I) fieter Results (mg/I )(m gikg) Organic Com pounds Results(m;;/1) P&T:GGMS antimony -l_) _ ::i.. -Jenzcr.e -Acid:B/N Ext. -i.--"1'seni c <7f -carbon tetrachloride I= 2,4-D --·-----_ l--, n,ri um -· 4L_ ___ -----·· __ , chlordane . --- 2,4,5-TP(Silvex) _ beryllium -cWoroben.zene -chlordane ~dmiurn <:,Jt) chloroform . - I= heptachlor -chloride o-cresol I /J(o - he:Xachlorobenze!:le ~omiurn rn-crc:.sol - hexachlorobutatjiene ~alt p-cresol -,4 - endrin pper cresol F - lindane fluoride 1,4-dichlorobcnzene -- methoxychlor iron ! ,2-dichloroethane ---</D - -toxapht::ne ~ad 1, 1-dichJoroethylene - I= -manganese -2, 4-dichloroethylene ~ercury .t_c, • .oP-, -heptachlor -::vi,;ckel 54 -bexachloroben.zene L. nitrate hexachlorobutadiene ~enium - ,L_ d. ~ hexachloroethane _2/0 -~ver -methyl ethyl ketone FOR LAB USE ONLY -sulfates nitrob~nzene late Received -- -thallium pentachlorophenol - -vanadium pyridine '2J2F - ~zinc -tetraChloroethy lene rate Extracted -pH trichlorot::thy lene - -conductivity -2,4,5-trichlorophenol Date Analyzed -TDS 2, 4, 6-trichlorophcno I - teported By -flash point -vinyl chloride ·-endrin -lindane -- Date Rtirf' ~ _ methoxychlor L ___ lJ::i2 AUG 1798 -- --toxaphene b Number • 2,4-D -- --2,4,5-TP (Silvex) r HS 3191 (Revised 11/93) I 'NC.:'DC}'anmcnt of En,..ironmcnt, Health, & Narural Ruources Solid Wut.e Management Divi,ion SMIPLE Ai'IALYSIS REQUEST SampldD Number/I State La.boratory of Public Hc.allh P.O. Box 28047, 306 N. Wilmington St. Ralcii:h. North Carolina 27611-3047 CD-012-SL 08/11/98 1720 GRAB 12345678 CD081098, NC o. WILSON INameofSite Cri ,,-t,;Y, Dev m s I ·fe-Collected By __ i~~~G-CLP HETALS Soil iteLoC.1tion __,,_fJ'-"X-1-lo..u.. .... G_,_("-j-+--,-l-(\,,_)_0"""'' ____ Date Collected ____ -;::::======----=--_:1::._4..:_:4 __ _ lteNumber /JC, 0 (20 / {oO0 d .<1J tgency: __ Hazardous Waste Solid Waste _0uperfund TCLP Compounds Sample Type I En_vironmental Concentr::ite Ground Water (1) Solid (5) L Surface Water (2) Liquid (6) .-Soil (3) Sludge (7) Other (4) Other (8) Organic Chemistry arameter P&T:GC/MS Acid:B/N Ext. 2,4-D 2,4,5-TP(Silvex) chlordane bepLachlor Results (mg/I) hexachlorobenzene _____ _ hexachlorobutadiene '-------- end ri.n lir.dane methcxychlor toxaphene L FOR LAB USE ONLY ate Rece!ved _________ _ rate Extracted _________ _ Date Analyzed _________ _ .eported By · Date Reported · I 01-_i_J_Gu-7 -AU_G_l_7_98- Lab Number IDHS 3191 (Revised 12/93) Comments Inorganic Chemistry Par";Jleter Results(mg/l)(mg/kg) _y antimony ,;__ 1 • ;J.. ~seruc __ L.:.~4~--- ·--t>)>,rtium _f5~0~-- -beryllium ~dmiurn __ <-~Io~--- chloride ~omiurn /:SD ~alt pper so fluoride iron ~ad <io -manganese ~ercury \ 4,0_c,5 ~ckel 1a nitrate ~eniurn ,;___ dJ ~Iver <-iD sulfates thallium vanadium ~zinc BB pH conductivity TDS flash point Inorganic CompoW!ds arsenic barium cadmium chromium lead mercury selenium silver Results(mg/1) Organic CompoW!ds Results(mg/1) benzene carbon tetr.:ichloride chlordane cWorobenzene chloroform o-cresol m-cresol p-cresol cresol 1,4-dichlorobenzene 1,2-dichloroethane 1, 1-dichloroethyleoe 2, 4-dichloroethylene beptachlor hexach.lorobenzelle hexachlorobutadiene ~ hexachloroethane methyl ethyl ketone nitrobenz.ene · pentachlorophenol pyridine tetraC:'hloroethylene trichloroetbylene 2, 4,5-trichlorophenol ------- ------- ------- ------- 2,4,6-trichlorophenol-'------- vinyl chloride endrin lindane methoxychlor toxaphene · 2,4-D 2,4,5-TP (Silvex) I NC,DcpJrtmcnt of Environment, Hc.alth, & Narural Ruourcc, Solid Wut.e M1.1ugcmcm Divi,ion SAMPLE ANALYSIS REQUEST St.ate Laboratory of Public Health P.O. Box 18047, 306 N. Wilmington St. Ralciyh, North Carolina 27611-8047 .Number Alto {!)0/ (oQ{p 2,C1J. SamplclDNumbcr C0-112-SL 08/11/98 1720 GRAB NameofSite Cri itex ·•· tkc, m ,5 ,-:j.:l, ~ll~t~By-=--~~:~5678. CD081098, NC D. WILSON - leLoc:ition {) )( 1-o c~ /\) G DateCollected . !NORG-CLP HETALS Soil , tency: --Hazardous Waste --Solid Waste 0uperfund TCLP Compounds 147 Sample Type Inorganic Compounds Results(mg/1) .Environmental Concentrate Comments arsenic - -barium Ground Water (I) Solid (5) cadmium --- l chromium - Surface Water (2) Liquid (6) -lead --mercury Soil (3) Sludge (7) -selenium r -silver - -Other ( 4) -Other (8) - -I - Organic Chemistry Inorganic Chemistry - tarneter Results (mg/I) ~e:er Results(mg/l}(mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS antimony < i. ?, benzene - -Acid:B/N Ext. ~nic z'-!--carbon tetrachloride t 2,4-D -~um eo --chlordane ··-··-···---····· .. ---··- 2,4,5-TP(Si!vex) _ beryllium -cWorobenzene chlordane ~mium. <ID chloroform -- r= heptachlor _ chloride i o-cresol - hexachlorobenzene ~omiurn /']::J. -m-cresol hexachlorobutadiene ~alt i p-cresol -- endri.n per 1 sw cresol F - lindane fluoride 1,4-dichlorobenzene --rnethoxychlor iron 1,2-dichloroethane -z,o - -toxaphcne ~earl -l, 1-dichloroethyleoe I= _ manganese -2, 4-di chloroetb y I eoe ~ercury .,__T, -c.:B heptachlor - -eke! 4 hexachlor6benzene - I=_ · nitrate hexachlorobutadiene ~enium -~:J.. ~ hexachloroethane - ~ver <.JD -methyl ethyl ketone FOR LAB USE ONLY sulfates nitrobenzene . late Received -- -thallium pentachlorophenol - -vanadium pyridine - ~c 98, -tetrachloroethylene r•te Extracted -pH trichloroethylene - -conductivity 2,4,5-trichlorophenol -Date Analyzed -TDS 2, 4, 6-trichlorophenol - leported By -flas_h point -vinyl chloride -·-·-endrin lindane -- Date Rrorted . -methoxychlor I O _iJG,~ AOGl798 - --toxaphene ..ab Number 2,4-D -- --2,4,5-TP (Silvex) I HS 3191 (R~vised 12/93) I I I I I I I I •• I I I I I I I I I I NCDEHNR Organics Lab: --Oi\'isi of Waste Management ' 1 ' uperfund·Section lnorganics Lab: l.--- □ Hazardous Waste Section □ Solid Waste Section CHAJN OF CUSTODY RECORD Project NameJ1n-.sf.,,'i Di---,,,1 m 5, 'f-e..... Site ID# (NCD#) Do I loo u 61Su SampledBy: /),.,hY)/A w;/.,ovi Location: 9£1•<~ N JS Sampler ID __________ _ Address: ~ u ,.-~ C Telephone:MJ -J53-Z-$D/ )(3~7 Date Sampled: g-fi-9,g' -~/J'-1/9 ( Time Sampled: _________ _ Sample Types: Soil~ Water~ Waste __ _ Other --- Field Sample Numbers co-oo '-/-51..... co-01 z.-5l tD-01?6-()) C.O--oz't-so CO-oo'(-SL C'o-013-Gw CD-pl'/-SL l!fJ-oZ'(-Si.J C-0-oolP (;cv.] Co-01'/-SD. CJJ -0/'15W c.o-o-zs--..5.D Co-oz '16-uJ Co-w2.-J . ..,,L~-- Co-03 o-G0 c..0-11 r-&--"w"------ eo _,,,'?,-,,) co-I21.-5,-, RelinquishedBy:1 ffJ!lh, -"-...1 (I ~i'/S,L__ ... 'Sirrnature'\ f J Received By: 1.lt1 l,1,C. M1\\/J di (Signaturb) Relinquished By: ___ ---'--------'--- 1sianature1 Received By: _______________ _ (Signature) Relinquished By:. _____________ _ 1Sionaturel Received By: _______________ _ (Signa<ure) - Results Reported: !/!tu/ ,:) 1'v':~~Wc:.__ __ (Signature)· /' Date: "8/14/qtlJ Time: ({ ~ <;, 2-, Date: 'o/Nf 4f!> Time: I/: 52.,, Date: Time: -----··--- Date: ----Time: . ___ _ Date: Time: -------- Date: Time: -------- Date: It cs~ 'fY Time: o/: '16 ~ /' . ..._, . r -,..-~ , NC._\)-:.r,.r1mc~t of Environment, H~lth, & Nawu.l Re.sources SA.l\1PLE A.t'IAL YSIS REQUEST St.ate Laboratory of Public He.allh P.O. Box 18047, 306 N. Wilmington St. Solid Vl.ut.c Mamgemcnt Division Ra!eii:h, North Carolina 2/611-8047 l;iteNumber /I/to 00 I loOic ol s-O SampldDNumt CD-002-GW 08/11/98 1250 GRAB , Rcc~,v:·r-o. 1 12345678 C0081098, NC D, WILSON C, ( ameofSite { 1n·5fl'x Drum ,st:, CollectedBy_' ORG-CLP SEp 08 · / VOA Ground Water 199g Site Location /') X ,lo r(. I /ii C-DateCollectea SUPcR,,·u2? --s/;L,,x...,,.,_-1-=~~--,-i--'-~---------;:::===-----~_:.:,.'.'.._!-!;lc','.''iiTT!..!_cC~r-!::!:,~c:,-,._. ~· -~ •. gency: H=rdous Waste Sample Type I EnvironmenL1l Concentrate Ground Water(!) .--Surface Water (2) Solid (5) Liquid (6) Solid Waste 1-Soil (3) Sludge (7) Other (4) Other (8) Comments i 1---~------'----, Organic Chemistry Inorganic Chemistry IPar":J)erer Results (mg/1) Parameter Results(mg/l)(mg/kg) VP&T:GC/MS \ = Acid:B/N Ext. antimony •= ~:1:~ TP(Silvcx) ---·-------- i -- 1= a 1- 1= 1= chlo,dane heptachlor hexachlorobenzene ------hexachlo ro but.ad iene ~----- endrin lindane methoxychlor toxaphene •~---------, I FOR LAB USE ONLY Date Received <,?-/$i-9'J'i/P(J)G .,) I Date Extracted _________ _ Date Analyzed fi'--/'if' ~"f "g-1}.j IReported~pge:-{ 1 Date Repoff?-3 / -'1 .f' ----. L:ib Number 982601 - - ---·- - - - - - - - - - - - - - - - - - - - - - - - - - arseruc barium ·-·-···--------·•·•·-·-·-beryllium cadmium chloride chromium cobalt copper fluoride iron lead manganese mercury nickel nitrale selenium silver sulfates thallium Vanadium z.inc pH conductivity TDS flash point TCLP Compounds Inorganic Compowuls Results(mg/1) arseruc -barium - cadmium -chromium -lead - -mercury selenium -silver - - --- - - Organic Compounds Results(mg/1) benzene -carbon tetrachloride -ch.lorclane ·-------------·· ·-· chlorobenzene - chloroform -o-cresol -m-cresol - -p-cresol cresol - -1,4-dichlorobenzene 1,2-dichloroethane - -1, 1-dichloroethylene -2, 4-dichloroetbylene -beptllchlor hexachloroben.zene -hexachlorobutadiene -~ hexachloroethane - -methyl ethyl ketone nitrobenzene - -pen tllcblorophenol -pyridine -tetrach.loroethylene -trichloroethylene -2, 4, 5-trichl oro pheno I -2, 4 ,6-trichlorophenol -vinyl chloride er;drin - lindane - -methoxychlor -toxapheile 2,~-D - -2,4,5-TP (Silvcx) I -I • • ., . ) ' NC J?epartmcm of Environment, SAJvIPLE Ai'IALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Hullh, & Nawn.I Re.source, Solid Wu~ M11ugcment Divi,ion Ralc:iyh, North c,.ro[ina 27611-8047 liteNumber Alto 00/ (oO& as-D lll'ameofSite Cn·sfl'x Drum ,'Site, Sample ID Num C0-006-GW 08/12/98 1000 GRAB , 12345678 CD081098, HC D. WILSON ~iteLoc:ition _ _,{),x....,.,_'f,_,fo~r~(/~ _ _,_,J/J~~C,-~•---DateCollected Collected By~ ORG-CLP VOA Ground Water 26 I tgency: --Ha=dous Waste --Solid Waste Duperfund TCLP Compounds Sample Type Inorganic Compounds Results(mg/1) I EnvironmenL1I Concentrate Comments -arsenic barium - -Ground Water (1) -Solid (5) cadmium -L -chromium Surface Water (2) -Liquid (6) lead - -mercury .-Soil (3) ·'. Sludge (7) selenium -- -silver Other (4),_i'~' Other (8) -·--- t - -Organic Chemistry Inorganic Chemistry --r~r Results (mg/I) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) _ P&T:GC/MS -antimony -benzene Acid: BIN Ext. arsenic carbon tetrachloride ---2.4-D --·: barium chlordane 1.-·· .. ---------··------··-·--·---·----·---------------------_, ________ .. --2,4,5-TP(Silvex) -beryllium -chlorobenzene -chlor~:me. cadmium chloroform -- I= heptaehlor chloride o-creso! --hexachloroben.zenl.! -chromium m-cresol I - hexac.h1oro buU!.diene cobalt p-cre.sol ---endrin ,·' cresol ~ •.~ copper 1: ' --lindane · ;, fluoride 1,4-dichlorobemene -- methoxyc_hlor-iron 1,2-dichloroethane --toxaphcne lead I, 1-dichJoroethylene -- I -manganese -2, 4-dich Io roethy lene -mercury -heptachlor nickel hexacWorobenzene ---t--nitrate hexachlorobutadiene -selenium ~ bexachloroethane --silver methyl ethyl ketone --FOR LAB USE ONLY -sulfates nitrobenz.ene IDate Received - <7-l 'l-ffY?, WG -thallium pentachloropbenol - -vanadium pyridine -zinc tetrachloroethylene --I Date Extracted -pH -trichloroethy lene &'-tf-1'6 17,j -conductivity -2 ,4,5-trichlorophenol Date Analyzed TDS 2, 4,6-trichlorophenol -- .Reported By -flash point -vinyl chloride --endrin linrlane --Date Reported --methoxychlor lub Number 982602 --toxaphene 2,4-D -- --2,4,5-TP (Silvex) I DHS 3191 (Rcvi~cd 12/93) . . . ' I 1 •,;. j ' NC pc-p1t,:11fi.nl of Environment, SMIPLE Al~ALYSIS REQUEST SL.ate Laboratory of Public Health P.O. Box 18047, 306 N. Wilmi:tgton SL Ralcit,:h, North Carolina 27611-8047 Hu.Ith, & Nuuri.l Resources Solid WHt.c Mar.agcmcnt Divii:ion I Al II j I , ~-, r-CJ C0-013-GW 08/12/98 1715 GRAB ite Number _.1c:c.'V...,1,,<-Q'""--"'0__,O"-'-~'o""'O""'(.._f---'e,,a"-'-'-:>c,_ "--Sample!D N, 12345678 CD08!098, NC D, -wILSON .rame of Site 1liteLoc.1tion C n',5 fl' X J) r Id m ,21 /4 < Collected By ORG-CLP VOA Q 'X /o,-('J /11 l---' I I DateCollecteu tgency: Haz2.Idous Waste Solid Waste _0uperfund ---- Sample Type I Environmental Concentrate Comments -Grouod Water (]) -Solid (5) L I Surface Water (2) Liquid (6) -.-Soil (3) r, Sludge (7) - ; Other('+)}.:', Other (8) -- -I Organic Chemistry Inorganic Chemistry ' 'r/2er Result.s (mg/I) Parameter Result.s(mg/l)(mg/kg) , ,;__, P&T:GC/MS -antimony ,I " Acid:B/N Ext, arscn.ic '' ---' 1:-2,4-D '.~i barium ----·-·-·-··········-····-··-·---.... ---·-·--·--··-····-·· .. 2,,;,5-TP(Silvex) beryllium - ch!ordac.e cadmium -- I heptachJ9r -chloride hex:i.chlorObenzeD.e chromium - hexachlor.9butadiene -cobalt endrin , <'.i' -copper I lindane ,; , ,, fluoride , ..... -methoxyCJi_lor iron - -toxaphene -load I= -manganese -mercury nickel --1-nitrate - selenium -silver -FOR LAil USE ONLY sulfates - IDate Received !J-/tJ-fY//1', /JJ.S -tha.lliurn -vanadium ---ZlllC - .Date Extracted -pH -conductiv,ity Date Analyzed 'F-r?-98'n4 -TDS I Reported By -fhsh point - -Date Reported - IL.ab Number 982603 - - -I DHS 3 19 ! (Revised 12/93) Ground Water 39 TCLP Compounds Inorganic Compounds Result.s(mg/1) arsenic -barium -cadmium - chromium -lead - -mercury selenium -silver - - - - - Organic Compounds Result.s(mg/1) benzene -carbon tetra.chloride -chlordane -------chlorobenz.ene -chloroform - o-cresol -m-cresol - -p-cresol cresol - -1,4-dichlorobenzeoe -1,2-dichloroethane -I, 1-dichloroethylone -2, 4-dichloroetbyle□e -heplachJor bexachlorobenzene -bexachlorobutadiene -~ hexachloroethane --methyl ethyl ketone nitrobenz.ene - -pent.achlorophenol -pyridine -tetrachloroethylene -trichloroethy lene -2, 4,5-trichlorophenol -2, 4,6-trichlorophenol --vinyl chloride endrin -lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Silvex) I ' ' ' 1 ,, I ' NC pcp•:unsent of Environment, Hull.h, & Nawral Ruourccs Solid Wutc Maro.1gcmcnt Divi,ion ( ameofSitc iteLocation ' 7 ( SMIPLE A.t'l"ALYSIS REQUEST State Labon.tory of Public Hea.llh P.O. Box 28047, 306 N. Wilmington St. Date Collected Ra!ciyh, North C1.rolina 27611-8047 C0-019-GU 08/13/98 1020 GRAB 12345678 C0081098, NC 0, WILSON UPGRADIENT FROM LAGOON ORG-CLP VOA Ground Water -. 119 tgency: Haz.u-doll5 Waste Solid Waste _0uperfund TCLP Compounds ---- Sample Type Inorganic Compounds Resull5(mg/l) I Environmental Concentrate Comments -arsenic barium -Ground Water(!) Solid (5) -cadmium --L , chromium -Surface Water (2) Liquid (6) -le.1d - -~ercury Soil (3) " Sludge (7) selenium .--· --silver Other (4)J/ - Other (8) ---- t -,, -Organic Chemistry Inorganic Chemistry - ' IP~r Resull5 (mg/I) Parameter Resul l5(m g/1) (mg/kg) Organic Compounds Resull5(.ng/l) _. -, P&T:GC/MS -antimony -benzene ;, ;~•·· Acid:B/N.Ext. arsenic carbon tetrachloride ---,, I= 2,4-D barium chlordane ........ ·•. ·····-·-·-· ···-• --·---·-· -·-·· -··· ... -------· ---· --------------------2,4 ,5-Tl'(Si!vex) -beryllium -chlorobenzene ' -chlord:ine · cadmium chloroform --- I= heptachlor chloride -o-cresol - hexachlorobenzene chromium · -n~-cresol - hexachlo~q,butadiene cobalt p-cresol · --- endrin .. copper -cn:sol I -lindane ·t,i.: -fluoride -1,4-dichlorobenz.ene methoxycl}lor iron· -1,2-dichloroethane - -toxaphene kad I, 1-dichloroethylene -- II= -manganese -2, 4-dichloroetbylene -mercury -heptachlor nickel hexachlorobenzene --- ii--nitrate -hexachlorobutadiene selenium ~ hexachloroetbane ---silver methyl ethyl ketone --FOR LAB USE ONLY sulfates nitrobenzene -I Date Recei v,ed - --thallium penta.chlorophenol J?-J'l-'1'?Vf;W6 - -vanadium pyridine _, -zinc tetrachloroethylene --I Date Extracted . -pH -tricbloroethylene ~-1'3-Cfg-n;J -conductivity -2 ,4,5-trichlorophenol Date Analyzed -TDS 2 ,4,6-trichlorophenol -I Reported By -flash point -vinyl chloride --endrin lindane --Date Reported --methoxychlor I Lab Number 982604 --toxaphene 2,4-D -- --2,4,5-TP (Silvex) I DHS 3191 (Revised 1'2/93) I r l' j NC _Dcpa.-1.n•.:nl oi Environment, Health, & Nawn] Re1oources Solid Wute M1111igcmcm Divi,ion SAMPLE Ai~ALYSIS REQUEST Slate La.boratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Raleiy~. North Carolina 27611-8047 lite Number ~N'-"-'<l-c.J' C...:.)---'0"'-"'DCJ_/ ~/4~o~O~&---=--i51'-5'-cc.._v_-__ Sample m N um C0-019-SW 08/13/98 1S30 GRAB 12345678 C0081098, NC 0. WILSON OOWNGRAOIENT FROH WETLAND ( ameofSite iteLoC'.ltion Cn·sfl'x Drl,fm ,'S>/c, ()_ x -fo,-r/ N l-- Collected By_ ORG-CLP VOA Surface Water ' -Date Collected 126 I tgency: H=rdous Waste Solid Waste 0uperfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) I Environmental Concentrate Comments -arseruc barium - Ground Water (1) -Solid (5) -cadmium -L \ -chromium Surface Water (2) -Liquid (6) -lead -mercury .-Soil (3) · t,, -Sludge (7) -selenium '. silver - -Other (4),;ii -Other (8) - I - -Organic Chemistry Inorganic Chemistry - r0&rer . Results (mg/1) Par:uneter . Result.s(mg/l)(mg/kg) Organic Compounds Result.s(mg/1) _. _ P&T:GC/MS -antimony -benzene ; .. Acid:B/N Ext. arsenic carbon tetrachloride --- I= 2,4:D ~i":'" barium ---chlordane . --·---·---·--·--·-·-·-..... , ... -·-·· -------· 2,4,5-TP(Silvcx) -beryllium -chloroben.zene chlordane cadmium chloroform ---- I hepwchl,or -chloride o-cresol - hexachlorobe=ize::ie -chromium -m-cresol hexachlorobut.adiene cobalt p-cresol -•,r,: -- endrin , copper cresol I ~-\ . -- lindane ·" · fluoride 1 , 4-dichlorobenz.e□e . ~ --methoxychlor -iron 1,2-dichloroethane - -toxaphene lead 1, 1-dichloroethylene -- ! I ·. manganese 2, 4-dichloroethy lene -- -mercury -hep"1chlor nickel hexachloroben.zene ---l--nitrate -bexachlorobut.adiene seknium ~ hexachloroethane --silver methyl ethyl ketone --FOR LAB USE ONLY sulfates nitrobenzene -I Date Received ?-/£/--ffl/e[J}G - -thallium pen"1chlorophenol - -vanadium pyridine - -zinc tetrachloroetbylene -I Date Extracted -pH -trichloroethylene 5?~J~-qg--7J;J -conductivity -2, 4,5-trichlorophenol Date Analyzed -TDS 2 ,4 ,6-trichlorophenol -I Reported By -flash point -vinyl chloride --endrin lindane --Date Reported --methoxychlor I Lab Number :·• tcxaphene· 982605 --2,4-D -- --2,4,5-TP (Silvex) I DHS 3191 (Revised 1::93) I ! ·, ,· . • • NC:: ,Depanmen1 of Environment, Hc.alth, & Nawnil R~ources SAMPLE Ai'IALYSIS REQUEST St.ate La.boralOry of Public Health P.O. Box 28047, 306 N. Wilmington St. ' .. •. ! Solid Wule Muu.gement Divi,ion Rali:it:h, Nonh Carolina 27611-8047 lite Number /I/to OD I /oO& a s-D Sample ID Nur C0-020-GW 08/13/98 0935 GRAB Crt-5fl'x IJ,um ,2itc, , 12345&78 C0081098, NC O. WILSON ( ameofSite iteLoca.tion tJ_ x for/'/ /II l--, l ( Collected By_ Date Collected - ORG-CLP l\gency: --Hazardous W a.ste --Solid Waste _0uperfund Sample Type I Environmental Concentrate Comments -Ground Waler(!) -Solid (5) L ' Surface Water (2) Liquid (6) -.--Soil (J) , .. Sludge (7) - -· Other (4)',J Other (8) -- I Organic Chemistry Inorganic Chemistry rar:JJ],efer Results (mg/I)· Parameter . Results(mg/l)(mg/kg) _XP&T:GC/MS -antimony VOA Ground Water 60 TCLP Compounds Inorganic Compounds Results(mgil) arsenic -barium -cadmium -chromium -lead - -mercury selenium -silver - - - - - Organic Compounds Results(mg/1) benzene -'" ., Acid: BIN Ext. arsenic c:irbon tetrachloridl! --- 1----2,4-D.~ ~w , __ -·-•--·--·-· ····-------··--·-b1rium ___ ,, ____ ,. ___ -chlordane ---------___ ,, ____ ,. 2,4,5-TP(Silvex) -beryllium -chlorobtniene --·---- E chlo~dane -cadmium -chloroform heptachlor . chloride o-cresol --hexachJorobe:uene -chromium -m-cresol bexachlor9butadiene cobalt p-cresol --endrin . copper cresol I --lindane'· >1 -fluoride 1,4-dichlorobenzcne - methoX:y~hJor iron 1,2-dichloroethane - toxapht!~e -lead -I, 1-dichloroethylene I -mangane~e -2,4-dichloroetby lene -mercury -beptachlor nickel hexachlorobenzene ---11--nitrate hexachlorobutadiene -selenium ~ hexachloroethane --silver methyl ethyl ketone --FOR LAB USE ONLY -sulfates nitrobenzene IDate Received - -thallium pentachlorophenol 15-/4'--9</"(tu!G - -vanadium pyridine -z.inc tetrachloroethylene --I Date Extracted -pH -trichloroethy lene o'-IC/ -q<j 71.:J -conductivity -2 ,4,5-trichJorophenol Do<e Analyzed -TDS 2, 4,6-trichlorophenol -I Reported By -fla.sh point -vinyl chloride --endrin lindane --Date Reported --methoxychlor lwb Numbe; 982606 --loxaphene 2,4-D -- --2,4,5-TP (Silvex) I DHS 3i9\ (Revised 11/93) I Ne _Dcp:~.!ne~t of Environment, He.alth, & Narural Re,ourccs Solid Wane Marugcmcnt Divi,ion SMIPLE Ai'IALYSIS REQUEST St.ate Laboratory of Public Health P.O. Box 18047, 306 N. Wilmington Sl. Ralei,;h, North _C1.rolina 27611·804] lite Num_ber -'/J-"--'-<(;,'-'[.,_) -'OL-"'D-'/'-"/o"-0"'-"'&----"-o<'--'S<-::,__D __ Sample ID Numl, CD-024-SW 08/10/98 1520 GRAB 12345678 C0081098, NC D. WILSON .rameofSite ~iteLoCJ.tion Cn·sfl'x Drum ,)J/4,, CollectedBy~ ORG-CLP ()_ X -/4 ,-r.l N' l--Date Collected ' I ( tgency: H=rdous Waste Solid Waste _0uperfund ---- I Sample Type Environmental Concentrate Comments -Ground Water (1) -Solid (5) L ' ' Surfar.e Water (2) Liquid (6) - ·-.-Soil (3) .,,:. Sludge (7) -' •\'. ~ Other (4)/; Other (8) -- I Organic Chemist,y Inorganic Chemistry [v?efer · Results (mg/I) Parameter Resulls(mg/l)(mg/kg) : . _ P&T:GC/MS -anlirnony l' 1,'' Acid: ll/N Ext. arsenic l "--I= 2,4-D b . barium ·-·-··-·-·--··-·-··-· .... -·--······· ·-·--·-···-------·-·---. 2,4,5-TP(Sihex) beryllium. - chiord:mc cadmium -I= heptachlor -chloride hexachlorobenzene -chromium hexachloro bu tad i ene cobalt -.,~---endrin '' copper ·,:' ' 1: -lindJ..11e .; • fluoride ' - methoxx~rlor iron - -toxaph~ne. . lead -- I -manganese -mercury nickel --1--nitrate selenium -silver -FOR LAB USE ONLY . sulfate·s - IDate Received -thallium g"--/1)-~tJG -vanadium z.inc - .Date Extracted• -pH '8-11-cz~m -conductivity Date Analyzed -TDS I Reported By -flash point - -Date Reported - I Lab Number 982607 - - -I DHS 3191 (Rcvi.sed 1:2/93) VOA Surface Water 76 TCLP Compounds Inorganic Compounds Results(mg/1) arsenic - barium -cadmium - chromium - le.1d - -mercury selenium -silver - - - - -- Organic Ccmpounds Results(mg/l) benzene -carbon tetrachloride -chlordane ---- chlorobenz.ene -chloroform -o-cresol - rn-cresol - -p-cresol cresol - -I 14-dichlorobenzene 1,2-<lichloroethane - -I, J-dichloroethylene -2, 4-dichloroethylene -heptachlor hexachloroben.zene -hexachlorobutadiene -. hexachloroethane - -methyl ethyl ketone nitroben2ene - -pentachlorophenol -pyridine -tetrachloroethylene -trichloroethylene -2, 4 ,5-trichlorophenol -2, 4, 6-trichlorophenol -vlI1yl chloride endrin -lindane - -methoxycWor -tox.aphene -2,4-D -2,4,5-TP (Silvex) I ' . . Ne' Depan~,rnt of Environment, SAMPLE A.t'l"ALYSIS REQUEST St.ate Labora\.Ory of Public Health P.O. Box 28047, 306 N. Wilmington St. Health, & f':'awral Resources Solid WuLC Mara.gcmcnt Divi,ion Ralcii:h, North C•rolina 27611-8047 lite Number Nt o O O I lo Ole oi s-O Sampk ID Number, C0-025-SW 08/10/98 1615 GRAB 12345678 CD081098, NC 0. WILSON · ,ameofSite ~iteLoc.'.ltion Cn·5 fl' X [) ru tr} ,-S>-/e, Collected By_·_· ORG·CLP Q x /4,0,/ NC-Date Collected ' I I lgency: --Haz.ardous Vv'aste --Solid Waste _0u per fund I Sample Type Environmenl'll Concentrate Comments -Ground Water (I) -Solid (5) L~ ' Surface Wate, (2) -Liquid (6) .. .-Soil (3) •11~ -Sludge (7) .. -Ot!:Jcr ( 4) t;; -Other (8) I Organic Chemistry Inorganic Chemistry ,tvrtt•r Results (mg/1) Parameter Results(mg/l)(mg/kg) · P&T:GC/MS -antimony '.. = Acid:B/N Ext. arsenic -I= 2,4-D . .;,~ ~ barium ------·-. -·--------------· -·-··· .. ---···-·· ··-····--··--·-· ....... 2,,1,5-T-P(Silvcx) -beryllium _ chlor_dane -cadmium I:= bept.ichlor -chloride hexa::hlorobenzene --chromium I bex:ichl0robu ta<liene cobalt I -' . -· _ endrin .:~ , ' copper -I= lind'1!1e .. , fluoride - -methoxy.<;.hlor iron - -toxaphene · -lead 1:--m:inganese -mercury nickel --t--nitrate selenium -silver - FOR LAB USE ONLY -sulfates .Date Received ?-/lf~JffV!j y}-6 -thallium -vanadium zinc - .Date Extracted -pH --conductivity Date Analyud 8~,9-~ -TDS .Reported By -flash point - -Date Reported - IL.ab Number 982608 - - -I DHS 3191 (Rcvi5cd 12/93) VOA Surface Water 83 TCLP Compounds lnorJanic CompoWlds Results(mg/1) arsenic -barium -cadmium --chromium - l""d - -mercury selenium -silver - - - - - Organic Compounds Results(mg/1) benzene -carbon tetrachloridt! -ch..lord.ane ----·--chlorobenune - chloroform -o-cresol -m-cresol - -p-cresol cresol - -1,4-dichlorobenzene 1,2-<lichloroethane - -1, 1-dichloroethylene -2, 4-dichloroetbylene -bept.ichlor bexachlorobenzene -bexachlorobutadiene - ~ hexachloroelhane - -methyl ethyl ketone nilrobenzene - -pentachlorophenol -pyridine -tetrachloroe-.thylene -trichloroethylene -2, 4,5-trichlorophenol -2, 4,6-trichJorophenol -vinyl chloride endrin -liridane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Silvex) l I NC Dep;d"~' of Env;ronm,n<, Health, & Narural Re.sourcci. SAivIPLE Ai~ALYSIS REQUEST St.ate LaboralOry of Public Health P.O. Box 28047, 306 N. Wilmington St. Solid Wut.e Mu:.1.gemcm Divi,ion Raleii,:h, Noi:h Carolina 27611-8047 liteNumber Nto 00 I loO& ol _s-0 CD-026-SW 08/10/98 1615 GRAB Sample ID Num~ 12345678 CD081098, NC D. WILSON jameofSite 'liteLoCJ.tion l'n-.5 f,,, X [) /IA tn ,,;~ ·le, '• : Collected By_': ORG-CLP {Y_ X forr/ NC--Date Collected ' 7 ( lgency: --H=rdous Waste --Solid Waste 0uperfund Sample Type I Environmental Concentr.ite Comments -Ground Water (1) -Solid (5) L ' Surface Water (2) -Liquid (6) . .-Soii (3) . ·,_, -Sludge (7) ,: -Other (4) p: -Other (8) I Organic Chemistry Inorganic Chemistry lar:uyeter . . Results (mg/I) Parameter Results(mg/l)(mg/kg) _1:::P&T:GC/MS -antimony Acid:B/N Ext. arsenic --· L ;:::~n'(Sil~ex) '-·-·-···-· ... ·--··-···----·--.. barium ' -·-···--···----·-beryllium -chlordane cadmium --I= heptach16r · -chloride hexachlorobenzene -chromium hexachlorobutadiene cobalt I= endrin ;;: : - -copper lindane , ·;. fluoride _ methoxy,liior - -iron toxaphene. -lead I= /, manganese - -~ercury nickel -- I= -nitrate selenium -silver -FOR LAB USE ONLY suifates Late Received - ?-/t/-7"6Vf?WG -thallium vanadium --zinc - rate Extracted -pH -conductivity Date Analyzed 8-JC, -c; ll-n.;J -TDS .Reported By -flash point --Date Reported - .Lab Number -982609 - -I DHS 3191 (Revised 12/93) VOA Surface Water 90 .l lu.J'-' TCLP Compounds Inorganic Compounds Results(mg/1) arsenic -barium -cadmium -chromium -le:1d - -mercury -seleniuµ:i silver - - - - - Organic Compounds Results(mg/1) benze'ne -carbon tetrachloride -chJordane ··--·· -----·-.. -· chlorobenzenc -chloroform -o-cresol - m-cresol - -p-creso.l cresol - -1,4-dichlorobenzene 1,2-<lichioroethane - -I, 1-dichloroethylene -2, 4-dichloroeth y lea e -heptachlor bexachloroben..zene -hexachlorobutadiene -~ hexachloroetbane - -methyl ethyl ketone nitrobenzene - -pentachlorophenol -pyridine -tetrachloroethylene -trichloroethylene -2, 4,5-trichlorophenol -2, 4, 6-t ri chJ orophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Silvex) . I •• J , NC Department of Environment, Health, & Nai;ural Reiourccs SAivll'LE Ai~ALYSIS REQUEST State L.a~orat_Ory of Public Health P.O. Box 28047, 306 N. Wilmington St. Raleii:h, North C1.rolina 27611-8047 I Solid Wute Management Divi,ion iteNumber Nto 00 I /oO!P a s-O rameofSite Cn'-5fl'x Drum ,21ie, SiteLocation r!J.. X /4,-1./ NC-- Sample ID Numb Collected By_ Date Collected C0-028-GW 08/12/98 1205 GRAB 12345678 CD081098, NC D. WILSON PERMANENT MONITORING WELL ORG-CLP ~OA Ground Water 130 ' I r - lgency, --Haz.ardou.s W a.ste Solid Waste .Duperfund TCLP Compounds -- I Sample Type Inorganic Compounds Result.s(mg/1) Environmental Concentrate Comments arsenic -barium -.-Ground Wat~r (!) Solid (5) cadmium -- ' -chromium Surface Water (2) Liquid (6) IC.1d --- -mercury 1--Soil (3) ' Sludge (7) I . ·\ --se.eruum silver ' -Other (4)~' Other (8) . -- l .. - -Orga·nic Chemistry Inorganic Chemistry -, f Paran;etl,r Results (mg/I) Parameter Result.s(mg/1) (mg/kg) Organic Compounds Result.s(mg/1) . ..J::::P&T:GC/MS -antimony benzene -,~ Acid: B/N Ext. arseruc carbon tetrachloride 2.4-D '¥ ---· barium chlordane " ·---·--·-·-·· .. ___ ------------·--··---·---· . --·---.. ----·---. -2,4,5-TP(Silvex) -beryllium -chloroben.z.ene chlordane -cadmium -chloroform II . ,. chloride heptachlor -o-cresol - hexachlorobenzene chromium rn-cresol -- -bexachl~~obutadiene cobalt I p-cresol -- !I endrin· :! -copper cresol - lindane · -, fluoride 1,4-dichlorobenzene , .. -- -methoxychlor -iron 1,2-dichloroethane - 1= toxaphene lead I, 1-dichloroethylene ' --,~ ., manganese 2, 4-dichloroethylene -- --mercury -heptachlor nickel hexachlorobenze:1.e 11= -- -nitrate bexachlorobutadiene -selenium ~ hexachloroetbane -- -silver methyl ethyl ketone - I FOR LAB USE ONLY -sulfates nitroben.z.ene - -thallium pt:ntachlorophenol </-/~ -9?11§ rv t; -Date Received -vanadium pyridine -z.inc tetrachloroethylene I Date Extracted --- -pH trichloroethylene -conductivity 2 ,4 ,5-trichlorophenol t-,q-qf 12.::l --Date Analvzed -TDS 2,4, 6-trichlorophenol I Reported ~y - -flash point -vinyl chloride --endrin lindane --I Date Reported --methoxychlor 982610 --toxaphene Lab Number 2,4-D -- -2,4,5-TP (Silvex) DHS 3191 (Revised 12/93) -I I t~C Dep'1r1•·r:!,;t of Environment, Hullh, & Narural Re£ourccs Solid Wu~ Man,1,gcmcm Divi,ion SMIPLE Ai'\'ALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Raleiyh, Nonh Carolina 27611-8047 liu:: Number ..... N"--"'1,,'-' o""'---"'0_,O<.....Ll~lo~0'-6=t1_olc_" _s-z.~O __ Sample ID Numbe: C0-029-GW 08/12/98 1510 GRAB -, 12345678 C0081098, NC O. WILSON lame of Siu:: Cn·.5 fl' x [} fl,{ m ,)J ie < Collected By_·_ PERMANENT MONITORING WELL ORG·CLP VOA Ground Water iteLocation rfJ. X /,;,_.,,/ N ~ Dau::Collected 134 , ---. -' I tgency: Hazardoll5 Wasu:: Solid W asu:: _0'u per fund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) I Environmental Concentrate Comments -arseruc -barium Ground Water(!) Solid (5) -cadmium -- L -chromium Surface Water (2) Liquid (6)_ -Je;id --m:rcury .-Soil (3) .. Sludge (7) selenium -- -silver Other (4)~/ Other (8) --- I -·· - -Organic Chemistry Inorganic Chemistry - Par::uneter Results(mg/1) (mg/kg) Organic Compow1ds Results(mg/1) r~r. Results (mg/I) : P&T:GC/MS antimony benzene --,. Acid:B/N Ext. arsenic carbon tetrachloride ---,_---2,4-D ,1,. .. -· --·---·-·--· --·-· . barium chlordane --··· ---·----· ·-·--- ---•-----~N 2,4,5-TP(Silvex) beryllium chlorobenzene --chlordan'e cadmiuru chloroform --- bep1'1chlor · -chloride O·cresol -J= hexachlorobenzene -chromium m-cresol -_ bexachlor.obutadiene cobalt p-cresol -, --endrin .. copper cresol E lindane ); · -- fluoride 1,4-dichlorobenzene --_ methoxycfflor -iron 1,2--dichloroethane -_ toxaphen'e· -lead I, 1-dichloroethylene - I= .. -manganese -2, 4-dichloroelhylene -mercury . -beptachlor nickel bexachlorobenzene ---l--nitrate bexachlorobutadiene -selenium ~ hexachloroetbane --silver methyl ethyl ketone --FOR LAB USE ONLY sulfates nitrobenzene -- IDate Received >(-J'l-9</V,itt/t;;, -thallium pentachlorophenol - -vanadium pyridine - -zinc tetrachloroethylene - .Date Extracted -pH -trichloroethylene ?{~ J0--9¥'. 7/..1 -conductivity -2, 4 ,5-tric hJ orophenol Date Analyzed -TDS 2,4 ,6-trichlorophenol - .Reported By -flash point -vinyl chloride --endrin lindane --Date Reported --methoxychlor ILab Number 982611 --loxaphene 2,4-D -- --2,4,5-TP (Silvex) I DHS 3191 (Revised 12193) . . ' ' I N~ D~ar:i,~ent of Environment, Hc.a.llh, & N1.rur1.l R~ourccs SMIPLE Ai'JALYSIS REQUEST . . State Labon.tory of Public He.a.Ith P.O. Box 28047, 306 N. Wilmington St. Solie' Wane Management Divi,ion Raleigh, North Carolina 27611-8047 liteNumber Nto 00 I (oOIP a s-D Cr/-sf,,,x Drum ,Sic, Sample ID Number C0-030-GW 08/11/98 1705 GRAB 12345678 CD081098, NC D. WILSON Collected By__ ORG-CLP tame of Site ~iteLoC.Jtion U f for('/ ( NC-Date Collected ' I tgency: H:uardous Waste Solid Waste 0uperfund ---- I Sample Type Environmental Concentrate Comments -Ground Water (1) -Solid (5) L ' Surface Water (2) Liquid (6) -.-Soil (3).' ' -Sludge (7) ' -Other (4),J -Other (8) I : Organic Chemistry Inorganic Chemistry .• P~r Results (mg/I) Parameter Results(mg/:) (mg/kg) '. _, _ P&T:GC/MS -antimony Acid:B/N Ext. arseruc -1---2.4-D .. ,;,: __ ,_,_ barium 2,4,5-TP(Silvex) ---•-----·-·-· ---•---· _, _, -·-·· -beryllium. _ chlordane -cadmium I= heptaclil9r -chloride hexachlOrobenzene -chromium hexachlo'robutadiene cobalt -.. - I endrin ' -copper llndane~11 -fluoride methoxychlor iron -toxaphene -lead I: . manganese --mercury nickel --1--. nitrate selenium -silver ·-FOR LAB USE ONLY ·-sulfates .Date Received <f-I 'I -c W#']AJ r:, -thallium -vanadium J z.i.nc - .Dale Extracted -pH -ConduCtivity Date Analyzed 'if~,;io-qg: f/.:1 -TDS I Reported By -flash point - -Date Reported - ILab Number 982612 -- -DHS 3191 (Rcvi5ed 12/93) VOA Ground Water 101 . TCLP Compounds Inorganic Com pounds Results(mg/1) arsemc -barium -cadmium -chromium -lead - -mercury sele:iiurn -silver - - - - - Organic Compounds Results(mg/1) benzene -carbon tetrachloride -chlordane ··-----------··· ··-chloroben.zene -chloroform -o-cresol -rn-cresol - -p--cresol cresol - -1,4-dichlorobenz.ene 1,2-dichloroethane - -1, 1-dichloroethylene -2, 4-dichloroetbylene -heptachlor bexachlorobenzene -hexachlorobutadiene - ~ hexachloroetbane - -methyl ethyl ketone nitrobenzene - -pentachlorophenol -pyridine -tetrachloroethylene -trichloroethy lene -2, 4,5-tricWorophenol -2,4 ,6-trichJorophenol -vinyl chloride endrin - lindane - -rnethoxychlor -toxaphene -2,4-D -2,4,5-TP (Silvex) SAi\1PLE Ai',TALYSIS REQUEST SLAte Laboratory of Public Hea\lh P.O. Box 28047, 306 N. Wilmington St. Solid Wut.e Ma:ugemcnt Divi,ion Ralci1:h, North Carolina 27611-8047 lteNumber Nto OD I lo0IP a s-D li':uneofSite Cn·sfl'x Drum ,2!ic< Sample ID Numbc C0-031-GW 08/11/98 1850 GRAB 12345678 C0081098, NC 0. WILSON Collected By_·_, '!iteLocation !1 ){ -for{/ 1 /ll l-DateCollected __ _,QL.., ... _ .. _,_,.-'----'-'-'-----1+~'-'----"""------ ORG-CLP · Haz.1rdous Waste Solid Waste _0uperfund Sample Type I Environmental Conce;itrate Comments Ground Water(!) _ Solid (5) I '. Surface Water (2) -Liquid (6) Soil (3) •' . Sludge (7) ~-•., - ' 0 0th (4f'1·· Other (8) er -t, • - t- 1---0-r_g•'-,a-n-ic_C_h_e_m_is_t_ry ____ ~--I-n_o_r_g_a_ru_' c_C_h_e_m_is_t_ry_~___, Acid:B/N Ext. ( ___ 2.4-D _,,°~ _ L 2,4,5-TP(Silvcx) chlordane Result, (rng/1) Para.>Tleter Results(mg/l)(mg/kg) . ·--------- -------- antimony, arseruc b.i.ri11m beryllium cadmium crJoride chromium cobalt coppe, fluoride iron ------I= heptacWor hexachlorobenzene -hexachl9robutadiene'------~ endrin · ·: .' I= lindane,;•J .: _ methoxY,_cnlor toxaphene: E---- l~------1 I FOR. LAB USE ONLY Date Received 7-N~ffygws .Date Extracted---------~ Date Analyzed ~6:~-_._@~7~-CJ~f_1);1~- IReported By Date Reported _________ _ .Lab Number 982613 IDHS 3191 (Revised 12/93) - lead manganese ______ _ mercury nickel nitrate selen.iurn silver sulfates thai!ium vanadium ZlDC pH conductivity -------TDS flash point VOA Ground Water 105 TCLP Compounds Inorganic Compounds arsenic - barium -cadmium -chromium -lead - -mercury selenium -silver - Organic Compounds benzene carbon tetrachloride -chlordane Results(mg/1) Results(mg/1) --------···· -· -------chJorobenze:1e -chloroform -o-cresol -m-cresol - -p-cresol cresol -1,4-dichJorobenzene -1,2-dichloroethane - -I, 1-dicWoroethylene -2, 4-dichloroethylene -heptachlor hexachlorobenzene -hexacWorobutadiene -.._ hexachloroethane -_ methyl ethyl ketone nitroben.zene - -pentachlorophenol -pyridine -tetrachloroethylene -tricb.loroethylene -2, 4, 5-trichl orophenol -2, 4,6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor ·-toxaphene 2,4-D - -2,4,5-TP (Silvex) I Nt D~~r1n .. :enc of Environment, He.Ith,&. Naru['l.l Ruource:s SMIPLE At'l"ALYSIS REQUEST St.ate Laboratory of Public Health P.O. Box 28047, 306 N. Wilmingtor\ St. Solid Wute Management Divi,ion Ralci1::h, North C&rolina 27611·8047 liteNumber Nto 00 I /oOIR ol s-O lfameofSite ~iteLocation CrJ-5f,,x Dr/,fm ,2/lc, Q x hr(,/ ti_c,, ' ' I Sampio!D Nun:, C0-032-PW 08/13/98 1308 GRAB • 1 12345678 CD081098, NC D. WILSON Collectw By_ POTABLE WELL ORG-CLP VOA Ground Water Date Collected 109 lgency: Hazardous Waste Solid Waste _Du.perfund TCLP Compounds ----- I Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments -arsenic '°'" ,,f 'Jy iMoi't U#, j:c barium - Ground Water (1) cadmium --I_ ·, -chromium Surface Water (2) -Liquid (6) Sa.1 _ -I ""d mercury -.-Soil (3) ,.·~; -Sludge (7) -selenium ' . silver - -Other (4)' . -· Other (3) - I - -Organic Chemistry Inorganic Chemistry - IP~r RcSults (mg/l) Parameter Res_ul ts(mg/l)(mg/kg) Organic Compounds ResulL5(mg/l} _ P&T:CC/MS -antimony b~nzene - Acid:B/N Ext. arsenic carbon tetrachloride --barium cWordane I I 1---2,4-D .,,1_. ------------·-·-·-· .. --. ····-~· ··--··---· .. --•·····-··-•·-------·•·•.I' 2,4,5-Tl?(Silvex) -beryllium -chlorobenzene chlo:-Can!! -cadmium -chloroform - 1: heptacrJor -chloride -o-cresol hexacWorobenzene -chromium -rn-cresol hexachlorribut.adiene cobalt p-cresol -·:t -- endrin ·-copper cresol I ' -- lindane ~;};• · fluoride 1,4-dichlorobenze□e --rnethoxvChlor iron 1,2-dichloroethane -.,..._., --toxaphen·e -lead -1, 1-dichloroethylene I _,;. '" -manganese -2, 4-dichloroethylene -mercury -heptachlor nickel hexachlorobenzene --- it--nitrate hexachlorobutadie□e - selenium ~ hexachloroethane --silver methyl ethyl ketone --FOR LAB USE ONLY -sulfates nitrobenzene I Date Receive,! - r-1ff-. rrvl? w G -thallium pentachlorophenol - -vanadium pyridine :;; -zinc tetrachloroethylene --I Date Extracted -pH -trichloroethylene &'-J.~-Cf?ni -conductivity -2 ,4,5-trichlorophenol Date Analyzed -TDS '.2, 4,6-trichlorophcnol -I Reported By -flash point -vinyl chloride --endrin lindane --Date Reported --methoxychlor I Lab Number 982G14 --toxaphene 2,4-D -- --2,4,5-TP (Silvex) I OHS 3191 (Revised 12/93) -- I Nt D~~r'l~cnt of Environment; Health, & Nawral Re..ourccs SMIPLE Ai'l'ALYSIS REQUEST St.ate Laboratory of ~blic Health P.O. Box 28047, 306 N. Wilmington St. Solid Wut.c Mmagemcnt Division Raleii;h, North Cuolina 27611·8047 Sample ID Nc C0-040-SW 08/13/98 1625 GRAB 1 12345678 C0081098, NC O. WILSON Collected By: liteNumber !Jto 00 I loO& ex s-D r=eofSite cri-.sfl'x Drum ,£/4, Site Loc:ition _ _.,cQ,:,c.-,,_X'-+fo-"--',---'--"~""'J,___~ 1 f-, _,_N--'-_,,C---cc 4 ___ Date Co llecte< ORG·CLP VOA Surface Water 138 Hazardous Waste Solid Waste _0uperfund TCLP Compounds Sample Type I Environmental Concentrate .-Ground Water (I) Surface Water (2) -Solid (5) -Liquid (6) Soil (3) ... -Sludge (7) Other (4):• ·-Other (8) Organic Chemistry 1r~1p __ ~_Ul P&;~Gc,~s ii Acid:B/N Ext. .~ 2,4-D ~ ... 2,4,5-TP(Silvex) chlordane heptachlor Results (mg/I) II= II= hexachlorobe112ene _____ _ hexachlorobutadiene "------- e_ndrin ±: ltndane.,fr rnethoxychlor toxaphene I FOR LAB USE ONL y Date Received ?-/<;i-';1}71/,o l{/6 ../ I Date Extracted--------,--~ Date Analyzed -~~~-J.~~--C,~&~?J~.J __ I Reported By 1 Date Reported Lab Number I DHS 3191 (Rcvi5cd 1:2/93) 982615 Comments Inorgan.ic Chemistry Parameter Results(mg/1) (mg/kg) -anlimony arsenic -barium --.. -·-·---·-·-·-·-·-··--- -beryllium cadmiuni -chloride -chromium -cobalt - -copper fluoride - iron -lead - -manganese -mercury nickel -nitrate -selenium -silver -sulfates -thallium -vanadium -zinc - -pH -conductivity TDS - -flash point - - . Inorganic Compounds arsenic -barium -cadmium -chromium -lend - -mercury selenium -silver - - - - Organic Compounds benzene - - - - - - - - - - - - carbon tetrachloride chlordane chJorobenzene chloroform o-cresol m-cresol p-cresol cresol I, 4-dichloroben.zene 1,2-dichloroethane 1, 1-dichloroethylene 2, 4-d ich 1 o roe thy I ene hept'1chlor hexachlorobenzene hexachlorobutadiene ..._ hexachJoroetbane -_ methyl ethyl ketone nitrobenz.ene - -penLachloropbenol -pyridine -tetrachloroethylene -trichlorot!th y lene ·-2, 4,5-trichlorophenol -2,4,6-trichlorophenol -vinyl chloride endrin - lindnne - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Silvex) Results(mg/1) Results(mgil) I Ne D~~rt~•~nt of Environment, Hc.ah.h, & Nawn.I R«ourccs SAMPLE Ai'l'ALYSIS REQUEST SlAte Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington SL Ra!ci1:h, North Carolina. 27611-8047 Solid Wute Management Divi,ion liteNurnber Alto 00 I loO& a s-O l 1n·sfl' x Drum ,S fc, ()_ X /4 r /',I . N C-- Sample ID Numb CD-102-GW 08/11/98 1250 GRAB 12345678 CD081098, NC D. WILSON . llfarneofSite ~iteLocation ' I I lgency: Ha=dous Waste ---- I Sample Type Environmental Concentrate Ground Water (I) -Solid (5) I_ ' Surface ~ater (2) Liquid (6) - ; . Collected By_ ORG'CLP Date Collected Solid Waste _0uperfund Comments 1-Soil (3) ,,_. -Sludge (7) -Other (4),". -Other (8) I Organic Chemistry Inorganic Chemistry IPv?,'.erer Results (mg/1) Parameter Results (m g/1 )(mg/kg) _ P&T:GC/MS -antimony Acid:B/N Ext. arsenic -1~--2,4-D ~ ---barium --. -··--·--·. ·-. -----······-····· - 2,4,5-TP(Silvex) -beryllium chlordane cadmium -- I= heptachlor -chloride hexachlorobenzene -chromiu~ hex:ichlorobutadiene cobalt --endrin . ' I < -copper lind.me .. r.:. -fluoride methoxy}~1hlor iron --toxaphene -lead I -manganese -mercury nickel -- 1[-. nitrate - selenium -silver -I FOR LAB USE ONL y -sulfates -thallium F-1t1-1rvtwG Date Received -vanadium zinc -I Date Extracted -pH -conductivity Date Analyzed x:-,;l..K-9 x -f/e'J -TDS I Rep~rted By -flash point - -Date Reported -I L:ib Number 982616 - . - -I OHS 319 I (Revised 12/93) VOA Ground Water 46 .. - TCLP Compounds Inorganic Compounds Results(mg/1) arsenic -barium -cadmium -chromium -le;id - -mercury selenium -silver - - - - - Organic Compounds Results(mg/1) benzene -carbon tetrachloride -chlordane. _,. ..... -·--------------chlorobenzen= -chloroform -o-cresol - m-cresol - -p-cresol cresol - -1,4-dichlorobenzene 1,2-dichloroethane - -1, 1-dichloroethylene -2, 4-dichloroethykne -beptachlor bexachlorobenzene -· hexachlorobuladiene -~ hexachloroethane - -methyl ethyl ketone n.ilrobenzene - -pentachlorophenol -pyridine -tetrachlorc :!thy lene -trichloroethylene -2 ,4 ,5-trichlorophenol -2 ,4, 6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5'.TP (Silvex) ·' I ·NC DCflan!n~nl of Environment, Hc.alt..'1., & Nawn] Ruourccs SA.i\lIPLE Ai~ALYSIS REQUEST SlAtc Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Solid ';,lane Ma·..agcmcm Division Ralci1;h, North Carolina 27611-80~7 liteNumber Alto 00 I /oO& 51 _s-0 Cr/·.sfl'x Dru1n ,c;>le< SampldD Numl Collected By_ DateCollecte<l , CD-126-SW 08/10/98 lblS GRAB 12345678 CD081098, NC D. WJLSON ta.me of Site ~iteLoc.J.tion cQ.x !no:/ NC--' I ORG·CLP - tgency: ·--Hazardous W a.ste Solid Waste Duperfund -- I Sample Type Environmental Concentrate Comments Ground Water(!) -Solid (5) I_: Surface Water (2) -Liquid (6) ~ Soil (3) •. , -Sludge (7) f Othe, (4)'.'· Other (8) --- I Organic Chemistry Inorganic Chemistry anu1J,.eter Results (mg/I) Parameter Results(mg/l)(mg/kg) .J::'P&T:GC/MS -antimony· Acid: BIN Ext. arseruc --· l= 2.4-D , ' barium -2,4.5-TP(Silvex) -·---··-··--·. •--·-·---····. . ....... --·•·---•------------- -beryllium chlordane · cadmium --~ beoLllcrJor -chloride hexach!orobenzcne -chromium _ hexachlc;)fobuc.adiene -cobalt I=. endri.n ,',' copper -lindane .~ -fluoride methox:i:chlor iron - toxaphene -lead I -manganese -mercury nickel --t--nitrate selenium -silver -I FOR LAB USE ONL y -sulfates -thallium ?---/'l-7W8'w6 Date Received -vanadium zinc - .Date Extracted -pH f-;;;i..~.-e;r :n<d -conductivity Date Analyzed -TDS I Reporte<l By -flash point - -Date Reported -lub Number 98261.7 - - -I DHS 3191 (Rc:vi.sed 12/93) VOA surface Water 97 TCLP Compounds Inorganic CompoWlds Results(mg/1) arsenic -barium -cadmium -chromium - le:id - -mercury selenium -silver - - - - - Organic Compounds Results(mg/1) benzene -carbon tetrachloride -chJordane -chloroben.zene -chloroform -o-cresol -m-cresol - -p-cresol cresol - -1,4-dichlorobenzene 1,2-dichloroethane - -1, 1-dichloroethylene -2, 4-dichloroethylene -hepLllchlor hexachlorobenzene -bexachlarobutadiene - ~ hexachloroetbane - -methyl ethyl ketone nitrobenzene - -pentachlorophenol -pyridine -tetrachloroethylene -trich1oroethy Jene -2,4,5-trichlorophenol -2,4 ,6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphene -2,4-D -2,4,5-TP (Silvex) I ' NC Department oi Environment, SAi\'1PLE Ai~ALYSIS REQUEST St.ate Laboratory of Public Health P.O. Box 28047, 306 N. Wilminb1ton St. Hcr..lLh, & Natural Resources Raleii::h, North Carolina 27611-8047 I Solid Wute Ma~gcment Divi,ion iu:Number Nto OD/ /oO{R ois-D lameofSiu: Cr/·,.-,fl' x Drum ,5>/c, Sample ID Nun; . I C0-100-TB 08/10/98 1630 GRAB 12345678 C0081098, NC 0. WILSON Collected By_ SiteLoc.stion {) X for (j /11 (,,-/ Date Collected TRIP BLANK ORG·CLP lgency: Hazardous W asu: Solid Wast<: _0uperfund ----I Sample Type Environmental Concentrate Comments .-Ground Water (1) Solid (5) - Surface Water (2) Liquid (6) --·, I-Soil (3) ', Sludge (7) - Othe: (4)·: Other (8) . I-- Organic Chemistry Inorganic Chemistry J"~r .. Re,;ults (mg/I) Parameter Results(mg/l)(mg/kg) _ P&T:GC/MS -anlimony ~ Acid:B/N Ext. arsenic - 2,4-D, .•-'" . -·-· • barium ·-------····-·--···--·-----·-··-2,4,5:TP(Silvex) beryllium --chlordane cadmium -F beptacli!or -chloride hexachlorobenzene chromium - hexa.chl~ 1 r~butadiene cobalt . -I== endrin ·, -coppe: lindane ): · fluoride - -methoxychlor -iron I= toxaphene -lead -manganese --mercury nickel I - -nitrate selenium -silver -I FOR LAB USE ONLY -sulfates -thallium l[-l~-7rveWG Date Received -vana'.}ium IDate Extracted -z.inc -pH _conductivity 8'-1-1-9~ 114 -Date Analvzed -TDS .Reported ~y -Ila.sh point - -I Date Reported - 982618 - Lib Number - -DHS 3191 (Revised 12/93) I VOA Other 148 · TCLP Compounds Inorganic Compounds Resull5(mg/l) arseruc -barium -cadmium -chromium - l""d - -mercury selenium -silver - - - - - Organic Compounds Results(mg/1) be:izene - carbon tetrachloride -chlordane --· ------~-·------cr'Jorobenzene -chloroform -o-cresol -m-cresol - -p-cresol cresol - -1,4-dichlorobenzene 1,2-<lichloroethane - -1, 1-dichloroethylene -2, 4-d ichloroethy 1 e□e -beptachlor -be.xachlorobenzene hexachlorobutadieoe - ~ hexachloroethane - -methyl ethyl ketone nitrobeniene - -pentachlorophenol -pyridine -tetrachloroethylene -trichloroethylene -2,4,5-trichlorophenol -2,4 ,6-trichlorophenol -vinyl chloride endrin - lindane - -rnethoxychlor -toxaphene -2,4-D -2,4,5-TP (Silvex) I t/C Dcjar!•rnent of Environment, Hc.allh, & Nawn] Resources SAMPLE Ai~ALYSIS REQUEST Slate LAboratory of Public Health P.O. Box 28047, 306 N. Wilmi%'1on St. Solid Wutc Ma:agcmcnt Divi,ion Ralci~h. North Carolina 27611-8047 liteNumber /ilto 00 I loO(f ol s-O ■<ameofSite Cn·5fl'x Drum ,2,:/c, Sample ID Num! C0-200-RB 08/11/98 1000 COHP 12345678 C0081098, NC 0. WILSON Collected By..:_ ~iteLoC"-tion_~O~~x~/4=·~-G~/~-~-~(1/-~C-~4 ___ DateCollected ...'. ORG-CLP VOA Rinsate 152 I lgency: Hazardous Waste Solid Waste _0uperfund TCLP Compounds ---- Sample Type Inorganic Compounds Rcsult.s(mg/1) I ~nvironmental Concentrate Comments -arsenic barium - Ground Water (1) Solid (5) -cadmiu·m --L ; chromium -Surface Water (2) Liquid (6) -lead - -mercury .-Soil (3) '" Sludge (7) selenium . -- -silver Other (4)1: Other (8) --- I - -Organic Chemistry Inorganic Chemistry - ,~r Results (mg/I) Parameter Result.s(mg/l)(mg/kg) · Organic Compow1ds Rcsult.s(mg/1) __ P&T:GC/MS -antimony benzene Acid:B/N Ext. arsenic carbon tetrachloride ---L 2,4-D ---·-·-barium . -·---·-----···---chlordane ·-----· ------·-·----·-------------······-··-· 2,4,5-TP\S11vex) -beryllium -chlorobenzenc chlordane cadmium chloroform -- I= heptachlor -chloride -o-cresol hexachloroben.zene -chromium -m-cresol hexachlorobutadiene cobalt p-cresol -. ' --i== endrin ,; -copper -cresol lindane ': -fluoride -1,4-dichlorobenzene methoxychlor -iron 1,2-dichloroethane -toxaphen~ - -lead I, l ·dichloroethylene - I= -manganese -2, 4-dichloroelhy le□e _. mercury heptachlor --nickel bexachlorobenzene --- I= -nitrate hexachlorobutadiene -selenium ~ hexachloroethane ' --silver methyl ethyl ketone --FOR LAB USE ONLY sulfates nitrobenz.ene IDate Received -- -thallium pentachlorophenol ?-/ ff. -'73'"1/§ W G - -vanadium pyridine -zinc tetrachloroethylene -- .Date Extracted -pH -trichJoroethylene 8'# .;n-9 <? fl{/ -conductivity -2, 4,5-trichlorophenol Date Analyzed -TDS 2, 4,6-trichlorophenol - .Reported By -flash point -vinyl chloride --endrin lindane --Date Reported --methoxychlor lub Number 982619 --toxaphene 2,4-D -- --2,4,5-TP (Silvex) I DHS 3191 (Rcvi:;cd 11/93) I tlC Dr!t'.Jar1•:lcnt of Environment, Hulth, &. Narural Ruourccs SAl'vIPLE Ai'l"ALYSIS REQUEST St.Ace Laboruory of Public Hc.a!th P.O. Box 28047, 306 N. Wilmington St. Solid ':I••~ M•r,..gcmcnt Divi,ion Raleigh, North Carolina 27611-8047 liteNumber /IJto 00 I (oO& a s-D r=eofSite { 1n·5ft"x Drum ,211e, Sample!D Nurn C0-400-08 08/14/98 1300 GRAB 12345678 C0081098, NC 0. WILSON Collected By_ DI BLANK SiteLocation _ _.,(Y_;;c...,,,,X~/4'-"'-"-r_,_;;"-/ __ 1 1--, .Lfl/--'-_,,,L--c::..._ __ Date Collected_ ORG-CLP Jgency: Hazardous W a.ste Solid Waste Sample Type I Environment.al Concentrate Ground Waler (I) -Solid (5) Surface Water (2) -Liquid (6) t-Soil (3) _ Other (4). -Sludge (7) -Other (8) _Duperfund Comments i----,-----'---, Organic Chemistry Inorganic Chemistry VOA water 158 TCLP Compounds lnorganic Componnds arseruc barium cadmium chromium lead mercury I • se,eruum silver Results(rng/1) 1Paral):)l'!'er r_V_P P&&lT:GC/MS Results (mg/I) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) F-Acid: BIN Ext. 2.4-D ,, 2,4,5-TP(Silvex) chlordane I= heptachlor hexachlorobenzene _____ _ hexachlorobutadiene 1= endrin • ,.: lindane :. _ rnethox.y~hlor t- ------ I FOR LAB USE ONL y Date Received 'fT--/'f-9![1(t, l{)6 IDate·Extracted _________ ~ Date Analyzed ~ -,;] 'i?-9 8:-o.;f .Reported By 1 Date Reported Lab Number 982620 I OHS 3191 (Revised ll/93) - - --- - - - - - - - - - - - - - - - - - - - - - - - - - anti.GJ.ony arseruc barium -·-·-------·-· ... ----·-· beryllium cadmium chloride chromium cobalt copper fluoride iron lead manganese mercury nickel nitrate selenium silver sulfates thallium vanadium zinc pH conductivity TDS !la.sh point benzene carbon tetrachloride -chlordane ·-·-chlorobenzene -chloroform -o-cresol -m-cresol - -p-cresol cresol - -1,4-dichlorobenzenc 1,2-dichloroethane - -I, 1-dichloroelhylene -2, 4-dichloroelhylene -beptachlor bexachloroben.zene -bexachlorobutadiene -... hexach]oroetbane -_ methyl ethyl ketone n.itrobenzene _ pent.achlorophenol _ pyridine -tetracbJoroetbylene -trichloroethylene --- -2, 4,5-trichlorophenol -2, 4, 6-t richl orophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphene -2,4-D -2,4,5-TP (Silvcx) ·-------. I I I I I I I I I I ~ I I I I I I I STATE LABORATORY OF PUBLIC HEALTH PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH, NC 27611 ORGANIC CHEMICAL ANALYSIS PURGEABLE COMPOUNDS LAB NO C/92-uO/ FIELD NO C.0-00 Z -&vi COMPOUND TYPE ( I l J, MDL~ (nnb) 9 ppm CHLOROMETHA.."IB :;. It) (,.L- VINYL CHLORIDE BROMOMETHANE CHLOROETHANE / TRICHLOROFLUOROMETHA..~ ' l,l·DICHLOROETHENE 0,5 ACETONE ;2,,0 IODOMETHANE [), 5 CARBON DISULFIDE METHYLENE CHLORIDE ACRYLONITRILE TRANS-1,2-DICHLOROETHE:'fE METHYL-t-BUTYL-ETHER 1,1-DICHLOROETHANE ISOPROPYL ETHER CIS-1,2-DICHLOROETHENE --' I 2-BlITANONE ;2,0 , .),, ' TETRAHYDROFURAN CHLOROFORM (),5 +race 1.1, l•TRICHLOROETHANE LA- CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE 1,2-DICHLOROPROPANE DIBROMOMETHANE , I ' I C- J - Possible lab contamination or background Estimated value K • L • 9~2(e02 9'2!2.C,,03 c.o-oo/r&w c.l> -013-e,<l ( ' l ( I l Q ppm e>ppm l.L (.,,L... 5.9 u__ ' I '1, B -r,L. 1,!S lL ' I (), &, u_ +ra..ce., frcu:.e., Ct,o, I l,L. '+ c.. · race.. l (.,,L... \ I I. I./- U-- \ I ' I qtc;2.lo04 962Uld5 o)-ol9-6W cD -01'1 ·Sv,/ ( I l ( J_ l 9 ppm 9 ppm u_ I I Yo.cs U-- ' I / ' J'f. 8 "J,c. r.;,., -r,c. I , I +ra.t:e, /J -'✓ +r('uP. lL +,~ I u_ ' I 3'-f,.(p I - 11fr11,..,~ 5,5-:r u.___, LL- \ 0,5 U,._ 2,5 u..., .,)/ 'I u - Actual value is known to be less than value given. Actual value is known to be greater than value given. Material was analyzed for but not detected. The number Not analyzed. is the Minimwn Detection Limit. NA - 1/ -Tentative identification. D -SAMPLE DILUTED. MDL'S DO NOT APPLY. DHHS 3065-1 (1/98) (0 9'o2LRD& cO-ozo-6-v-J ( ' l G0ppm 11 ' J --&;. 9 :s,c... / I - ,✓ fy()f'P .l / " PURGCOM2.ORG STATE LABORATORY OF PUBLIC HEALTH I PO BOX 28047 • 306 N. WILMINGTON ST., RALEIGH, NC 27611 ORGANIC CHEMICAL ANALYSIS PURGEABLECOMPOUNDS LAB NO 9621DOI Q62/JiOJ.. <1'i32lPO 3 q<c,Z.Co04 o/8 Z(J){J5 FIELD NO ~ COMPOUND TYPE ( I l ( I ) ( I l ( I ) ( ;2..) .MDL .. A ppm 8 ppm B ppm 8 ppm (9ppm (ppb) ~ BROMODICHLOROMETHA.'IE o.5 LL u.__. t.,L I l l CIS·l,3-DICHLOROPROPENE ,11 . I/ . ..L~,--.!/ ·, / f-;(lrP l/ , I 4•METHYL-2·PENTANONE 11.(f .,r I TOLUE!'i'E +m,.,.. +race.. +r(lrP +rnrP I TRANS-1,3-DICHLOROPROPENE u... u.__, I! I I . J, 'I ,/ 1, 1,2-TRICHLOROETHA...."iE TETRACHLOROETHE:-t'E +l"oc.e.. o.5 :r 0,8 +,,If,-I, U-+vacp .1.1 ~ 2-HEXANONE DIBROMOCHL-OROMETHANE (,.,L. +-r art>.!J LL ETHYLENE DIBROMIDE -!,,-I 'I • ,I I CHLOROBENZENE d•5 o.7 ~ l, 1, 1,2-TETRACHLOROETHA..'IE I , I I ETHYL BE:iZENE Ji t(ac.e.., I XYLENES I. 4-o.9 11 STYRENE J I I BROMOF'ORM. 1, 1,2,2-TETRACHLOROETHANE I 1,2,3-TRICHLOROPROPANE ,I 1,4-DICHLOROBENZENE +.,(Jr P . I I 1,2-DICHLOROBENZENE ,; I 3.1 +race.... J.,0 ,/ / ' .. ., I LL--'/ l.2,•DIBROM0•3·CHWROPROPANE I I C -Possible lab contamination or background. I J~ -Estimated value Actual value is known to be less than value given. -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. The number NA -Not analyzed. is the Minimum Detection Limit. 11/ -Tentative identification. D -SAMPLE DILUTED. MDL'S DO NOT APPLY. DIIBS 3065-2 (1/98) I Q8Zloo(p ( I ) eppm I I . • f., . I --fr'(fce.:u ', 'I/ .J-,;.,-, · p l/ . C ,. , ' I 9Co,3 l I ,J-y-/1 rO ICii,7 u__ PURGCOMZ.ORG '' ' STATE LABORATORY OF PUBIJC HEALTH I I PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH, NC 27611 ORGANIC CHEMICAL ANALYSIS I PURGEABLE COMPOUNDS LAB NO ct5zwo7 FIELD NO CD-o,~·S>N I COMPOUND TYPE I ;2 J .J, MDL } (~ ppm (nub) I CHI.OROMP:THAN'E ;}..,0 I J I VINTL CHLORIDE I BROIIO~ CHLOROETHAN?: I TRICBLOROP'LUOROME:THANE ' I l. l • Orem.a ROETH?:!tt a.5 ' I I ACrTOl<E 2,0 7,5JI-- 10DOKETHANE c.5 I I I CARBOl'f DlSUL11DI!: I M:rT'HTl.El'f1! CHLO RIDE I I ACRTI.O?'IT'I'RILZ I I TRA."fS-l.~DICHLDROETH?:~ I KrTBTL-t•BUTTL-ETH?:R I I t. l•Dlcm.oROrrli.,\ltt I I I I ISOPROPTL~ I CIS-1 ~DICHLORO~"l'E ~ 2•0 :i-eUTANONE I T?:I"RAHTDROP'URA!' ,1, CHLOROFORM o.5 I 1.1.1 · TR.I cm..oRQ rTlL\Nl: I CARBON' TrTR.ACHLORIDE I I 81!:NZ?:ffE I 1.2-DJCHLORO!:nlAlR I TRICm.08.0?;THE?ff; I l.2•D1CHLOROPROPAN'!: , ,I \ DIBROMOIIETHAN'E I C • Poaalble lab contamination or backgroand J -bCimat■d valu■ qsztoC0 C 0·tZ5-S\II I ;;:L J 9 ppm I 1 I I , IC -J.ceual valu■ i• known to b9 l■ • • than 'n.lu■ gi._n. qgzWA co-oii.-sw ( .;i.. J @ppm 11 , ._/ q,8:5,C Ii . ,,; 9'c32lPIO 902.li>II CO-o2S-6w co-ozq-6-w ( I J ( I J r9ppm @ppm I 1 I I l,5j LL. / , '75.3 I ,0 4-,1.,_---s; t.f,5-s,c I I LL, \ I ' / -1--rac.e.-/. B I I LL- 1,9 +(f11'"P u__ LA- 31,7 160,6 4, 1;,::Si I ( 1 -,/ ID, I }nice. l I , I I I _ 4.7 J_,, +,ace.. o.7 -j--vf"l[P +rac-' 57,9 '7r'/. 0 I I +,,,ce... ,I/ LL- O ---t■ria.l ••• analys■d tor but aot dat ■ct.■d. '%'b■ a~r 1■ th■ Ni.nimua D•t■ction LJ.JIIJ.t. I L -J.c:tua.l valu■ i• Jcnown to b■ gr■at ■r than Ta.lu■ giv■n. ID. -l!lot analysed. · l/ -hntatiT• id■ncitication. 0 -UIIPL& OII.OTJa). IIDL' 8 DO l!iJ0"1' APPLY. I DHBB 3065-1 (1/98) 9eZlol 2 C0 ·D3c-Gv/ ( I J g--ppm I I 1/C/,{p:r I I , r 3,'f 3, 3 -s,c. LL I I ' / Io, I LL O, l.P U-- 34-0, l.o; LL- J,, +-race. I .]/ +race.. +(11rP .527.l:r U-- Jt PtlllGCOM2.0RG , ' . STATE LABORATORY OF PUBLIC HEALTH I I PO BOX 28047 -306 N. WILMINGTON ST .• RALEIGH, NC 27611 ORGANIC CHEMICAL ANALYSIS I PURGEABLECOMPOUNDS LAB NO 461&o1 qs21oo<i3 FIELD NO I COMPOUND TYPE ( ;2 l ( ;l. l e ppm e ppm i" MDL.J, I (nnb) BROMODICHLOROMETHANE o.5 LL-J J -,II ,i/ I CIS•l,3-DICHLOROPROPENE +ma:ll t ,( . 4-METHYL-2-PENTAJiONE TOLUENE 1 · I +l("t1rP I TRANS-1,3-DICHLOROPROPENE IA__, l, l,2-TRICHLOROETHA.."iE I TETRACHLOROETHENE ,/ ' I --l-r11rc'.-.11 +mce.J.r 2·HEXANONE I DIBROMOCHLOROMETHA.."iE I l _ 1 • I ·~- \I I \I I ETHYLENE DIBROMIDE I CHLOROBENZEXE +race c... +((lrP C, l, l, l,2-TETRACHLOROETHA.."iE LL I l I ETHYL BENZENE XYLENES STYRENE I BROMOFORM l,1,2,2-TETRACHLOROETHANE I 1,2,3-TRICHLOROPROPANE 1,4-DICHLOROBENZENE I l,2-DICHLOROBENZENE ' I :J.,O ' I ' I l,2,·DIBROM0·3·CHLOROPROPANE I I I CJ -Possible lab contamination or background. -Estimated value K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. The number is I NA -Not analyzed. 11 -Tentative identification. D -SAMPLE DILUTED. MDL'S DO NOT APPLY. DHHS 3065-2 (1/98) I qg2,[pcA CiB::2-(1'/o qB2uil I ( ;L. l ( I l ( / l 8 ppm 8 ppm 8 ppm I I I I \/ I _u-.I ,/ ·-,y,11.,... +n1rP +r-ac"' ./-y(' r,:, I I u__ LL- I ,0 -!,, ,,,... 3;3, (oJ /If 0,5 trQceu +("ll(f' l/ +ran)/ I J Ll._ . ti ,u Jr J, +rnrP c... +roce. e, 10,5 I J 0,5 I J I I .L I --l, -, ' ~ - I I 8,3 111, '7 ' I \ I u__ the Minimum Detection Limit. Q8Zul2 ( I l 8'ppm LL-- . I +ra.ce.. I e,1,0 u.__ . I +ra.ce- I I ·• I 1,0 u..,., PURGCOM2.0RG STATE LABORATORY OF PUBLIC HEALTH I I PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH, NC 27611 ORGANIC CHEMICAL ANALYSIS PURGEABLE COMPOUNDS LAB NO 9'62wl3 FIELD NO C.l)-OoT-6\, COMPOUND TYPE ( / ) J, MDL+ (nnb) 3 ppm CHLOROMETHANE ;2,0 U- VINYL CHLORIDE J,(p I BROMOMETHANE I l CHLOROETHANE I TRICHLOROFLUOROMETHANE ' I '/- o.5 /G,, fJ l,l•DICHLOROETHENE I ACETONE ;2,0 3.f3°5•(. IODOMETHANE t),5 I, CARBON DISULFIDE J,, I METHYLENE CHLORIDE s'-1-,B ACRYLONITRILE / J I TRANS.l,2-DICHLOROETHENE METHYI,.t-BlJTTL.ETHER ,/ 1,1-DICHLOROETHANE Ci, ,":) ISOPROPYL ETHER I l CIS--1,2-DICHLOROETHENE \ I 55. ::Z. 2-BUTANONE :z.o I J TETRAHYDROFURAN J,, \I/" CHLOROFORM {) ,fi -1-.--ri Ce.. 1,1,l·TRICHLOROETHANE :2. 2- CARBON TETRACHLORIDE LL BENZENE +v-11 r,o I 1,2-DICHLOROETHANE LL. 14'7.")-TRICHLOROETHENE I 1,2-DICHLOROPROPANE I J \ / .Ji DIBROMOMETHANE I C -Possible lab co:ntaminatlon or background J -Estimated value q 8 Z(o J '-/- Cf>-032:-P'N ( ;)._ ) ~ ppm LL ,I ,:L.5 3,c. u.... O,ID c. LL ,I +,-o.c.e +-r"'c.e.y u__ I ' I K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. qf3z4i I 5 co-D'I0-5W ( /) ) 9 ppm I I ,/ ?. ''7 -s,c. L-L O,IJJ c... I I \ I 9826>/lo qszh17 CD•lbZ.-G-W C0·/2<,,-51;/ ( I ) ( ;;i. ) c@ ppm ~ ppm I l l.,L ,V 4.9 J,(. l-L. 0,5 c., 1 ,/ +-ll"" r e_. . +rc:v·P .!/ I I \ I +-,ArP 1 ., / '1/ I U -Material was analyzed for but not detected. The number is the Minimum Detection Limit. NA -Not analyzed. 1/ -Tentative identification. D -SAMPLE DILUTED. MDL'S DO NOT APPLY, I DHHS 3065-1 (1/98) qg 2(p/ £3 CP-too··TB ( .., ) ~ ppm L-L 'I 5;0 I 1 ., / PURGCOM2.0RG ' , STATE LABORATORY OF PUBLIC HEALTH I PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH, NC 27611 I ORGANIC CHEMICAL ANALYSIS I PURGEABLE COMPOUNDS LAB NO qgzu13 C/62-wl'f FIELD NO I COMPOUND TYPE ( I ) ( .?-. ) ,tMDL~ ~ppm 9 ppm I (nnb) BROMODICHLOROMETHANE 0,5 LL l,L. I CIS-1,3-DICHLOROPROPENE 4-METHYL-2-PENTANONE I TOLUENE TRA.'1S-1.3-DICHLOROPROPENE ,/ 1, l,2-TRlCHLOROETHANE +v00°. TETRACHLOROETHENE '80,'7 ~ 2-HEXANONE u_ DIBROMOCHLOROMETHANE , ETHYLENE DIBROMIDE . CHLOROBENZEN'E +(QC.P. 1, 1, 1,2-TETRACHLOROETHANE ( I ~ ETHYL BENZE:VE XYLENES STYRENE BROMOF'ORM -1, 1,2,2-TETRACHLOROETHANE 1,2,3-TRICHLOROPROPANE 1,4-DICHLOROBENZENE I 1,2-DICHLOROBENZENE ,; :2,0 ' ' 1,2,-DIBROM0-3-CHLOROPROPANE I I I C J - K Possible lab contamination or background. Estimated value Actual value is known to be less than value given. Actual value is knovm to be greater than value given. L qgz01!5 ( .l-.) sppm I I _ ,/ +vi> rP ' I I ,/ qgz{fl If.ti 9£32-4;/7 ( I ) ( .?-. ) cB ppm 8 ppm I J. I I ,I✓ ' , +f'nr<> l/ +r-QrP _1/ +rnrP -/--,,-r, CF' 1 I I ,/ ' / +rcVP~ +rrac~ I , I I , ' I ./ u Material was analyzed for but not detected. The number is the Minimum Detection Limit. I NA Not analyzed. 1/ -Tentative identification. D SAMPLE DILUTED. MDL'S DO NOT APPLY. DHHS 3065•2 (1/98) I qszu18 ( '-/) Bppm. LL- \ / PURGCOM2.0RG I I I I I I I I I I I I I I I I STATE LABORATORY OF PUBLIC HEALTH PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH, NC 27611 ORGANIC CHEMICAL ANALYSIS PVRGEABLE COMPOUNDS LAB NO CJ 6.2.1.,, /9 FIELD NO co-:i.oo-R•3 COMPOUND TYPE ( 'I ) ~ MDL ... (nnb) eppm CHLOROMETHA."IB ;2 ,t) 11 VINYL CHLORIDE BROMOMETHANE CHLOROETHA.'"iE TRICHLOROP'LUOROMETHANE \ I 1,l•DICHLOROETHENE o,5 ACETONE ;2,0 IODOMETHANE D,5 CARBON DISULFIDE METHYLENE CHLORIDE ACRYLONITRILE TRANS--1,2-DICHLOROETHENE METHYL-t·BUTYL-ETHER l.l•DICHLOROETHANE ISOPROPYL ETHER CIS-1,2-DICHLOROETHENE \ I 2-BUTANONE 2,0 TETRAHYDROF'URAN J,, \ I CHLOROFORM o.5 +r'OJP 1, l, I-TRICHLOROETHANE l.,L- CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE . TRICHLOROETHENE 1,2-DICHLOROPROPANE DIBROMOMETHA..'"iE ' I ._ I J - Possible lab contamination or background Estimated value qgz(o:ZO CD-'-loo-Di3 ('i ) 8ppm 11 ' I J,8 :r,c... U- o.7~ L.A.-- ' ' ' I I -I r /J ' I K - L - Actual value is known to be less than value given. Actual value is known to be greater than value given. ( ) ppb ppm ( ) ( ppb ppm ppb I Material was analyzed for but not detected. The number NA -Not analyzed. 11 -Tentative identification. D -SAMPLE DILUTED. MDL'S DO NOT APPLY. u is the Minimum Detection Limit. I DHHS 3065-1 (1/98) ) ( ) ppm ppb ppm PURGCOM2.ORG STATE LABORATORY OF PUBLIC HEALTH I ' . PO BOX 28047 · 306 N. WILMINGTON ST., RALEIGH, NC 27611 I ORGANIC CHEMICAL ANALYSIS I PURGEABLECOMPOUNDS LAB NO Cf6ZCDICf qg2uzo FIELD NO I COMPOUND TYPE (4 ) ( 4-) .. MDL~ t9 ppm Gppm I (oob) BROMODICHLOROMETHANE 0,5 u_ u I CIS•l,3-DICHLOROPROPENE J,,- 4-METHYL-2-PENTA.'iONE ../-Y fl r P .1,- ~ TOLUENE +rt1rP TRANS-1.3-DICHLOROPROPENE LL- l, 1,2-TRlCHLOROETHANE TETRACHLOROETHEm: ~I '/ -2-HEXANONE .J-,,-.ue.. Jr .Jy,., [P .l/ DIBROMOCHLOROMETHA."IB u._, I J ,u, ETHYLENE DIBROMIDE I CHLOROBENZENE +ra..c.P. l, 1, 1,2-TETRACHLOROETH.A.NE LL I ETHYL BENZENE XYLENES I STYRENE BROMOFORM 1.1,2,2-TETRACHLOROETHANE I 1,2,3-TRICHLOROPROPANE 1,4-DICHLOROBENZENE I ' I 1,2-DICHLOROBENZENE :J.,O \ ,/ 1,2,-DIBROM0•3·CHLOROPROPANE I I I C -Possible lab contamination or background. J -Estimated value K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. ( ) ppb ppm ( ) ( ppb ppm ppb U Material was analyzed for but not detected. The number is the Minimum Detection Limit. I NA -Not analyzed. 1/ -Tentative identification. D SAMPLE DILUTED. MDL'S DO NOT APPLY. Dlil!S 3065-2 ( 1/98) I ) ( ) ppm ppb ppm PURGCOM2.0RG r; 1 · .. ~c:g.,;,'.~ment o;Env;ronment, SAIVIl'LE Al'l'ALYSIS REQUEST State Labo.-.toty of Public He.ollh · Hui·i1, & N•rural Resources P.O. Box 28047, 306 N. Wilmington St. So[i,i Wu~ Marugcment Division Raleii:h_. North Carolina 27611-8047 l;i1eNumber fti'l;'i) OD I r; V (o 2 s-::n Sample!D Num CD-002-GW 08/11/98 1250 GRAB _J_ . . , 12345678 C0081098, NC D. W.Jl.SPJl:CEIVEO INameofSi1e Cr(<,fl'Y ,/)01 I:;:) ,5;!: ,Collected By~ ~ {£, 0RG-CLP EXT /PCB Ground ~f.p OB 'll'IAI\ Si leLoc:ition _,V"-' _,'/'-'-·fr,=) r,'4.~f.-·-i· _ ___,_/1/-'--'(.,_=----Dale Collecied _ 1;:J~O ■. . ~ ~r 1pr.::,:,r:, ,, , .... ,,.,,.~.,.."N rgency: --Hazardous Wasle --Solid Wasle __JcC>Uperfund TCtP' Ccimpouno.s Sample Type I Eu-vironmental Concentrate 1 Ground Water (!) Solid (5) 1-Surface Wate;· (2) = Liquid (6) 1-· Soil (3) Other (4) Sludge (7) Other (8) Comments Inorganic Compounds Resulls(mg/1) arsenic -barium -cadmium -chromium -lead -- -mercury selenium - silver - -1----------< - Organic Chemistry Inorganic Chemistry - IParameter P&T:GC/MS -~id:B/N Ext. I:,._-_-. 2 .4-D I 2.4,5-TP(Silvtx) chlordane Results (mg/I) I' hept.achlor hexachlorobenzc:1e _____ _ hexachlorobutadiene •·-endrin lindane .--methaxychlor toxaphene '_k:" PCB :> ------ FOR LAB USE ONLY I Date Received ?-/ t/-ff r;tuc · f'!(Ss y-t7·1'111i I Dat.e Extracted,6',IJJI 'f{-r7-9Y{{l!R,Jl'II ,}::/JI 8/J~ ff-i 8'-f K '/3J:J Date Analyzed pees 'i/-19-W-VP I Reported (;'"' i--J? ,O_ yl •"" 1 Date ReporteW_,,_f_~_3_c/_--4tf'-><--- Lab Number 98Z582 Parameter ResulLS(mg/l)(rng/k,'.) -- antimony ursemc barium berylliurn cadmium chloride ch1-.1miurn cobalt copper fluoride iron lead ma.nganese ______ _ mercury nickel nitrate sclen.iurn silver sulfates thallium vanadium zinc pH conductivity ______ _ TDS flash point Organic Compounds benzene carbon tetrachloride -chlordane Resu!L,(mg/1) -·--· -·-·-------··-·----·· chlorobcn.zenc --chloroform --o-cresol -m-cresol - -p-cresol cresol - -l ,4-dichlorobenzene 1,2-dichloroethane - -I, 1-dichloroethylene -2, 4-dichloroelbylene -heptachlor hexachlorobenzene - hexachlorobutadiene -""-hexacWoroethane -_ methyl ethyl ketone nitrobenzene - -penta.chlorophenol -pyridine -tetrachlo roe thy lene -trichloroethylene -2, 4,5-lrichlorophenol 2,4, 6-1richlorophenol -- -vinyl chloride endrin -lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Silvex) I I· , :"C Dc;,;nmcnt oiEnv;ronmcnt, . SMIPLE At~ALYSIS REQUEST St,tc Labo«tory of Publ;, Haith , Hc.a.";h, & N1.wral Re.\ourccs P.O. Box 28047, 306 N. Wilmington St. Solid Wute Management Divifiion Raleigh.' Nonh C1.roli.na 27611-8047 lite Number f;; D Oo I fe D (o 2 .:;:n Sample ID~ CD-006-GW 08/12/98 1000 GRAB C -_j_ 7' :C:f. 1 12345678 C0081098, NC D, WILSON l'lameofSite ~(Sjl'Y~ ,ur;~✓:, <.di-{£, _Co!lectedB, ORG-CLP EXT/PCB Ground Water 28 Sitel.oc:ition V '{f7i!cc,, fJ!_ L----DateCollect ~~~~~--+--~-~----.-----------------~ .gency: __ Hazardous Wa.ste __ Solid Wa.ste ~und Sample Type I Environmental J Ground Water(!) r Surface Water (2) 1-Soil (3) Other (4)_,' Concentrate -Solid (5) -Liquid (6) -Sludge (7) -Other (8) Comments J------- Organic Chemistry Inorganic Chemistry IPar:uneter Results (mg/I) I _ P§:T:GC/MS _!Acid:B/N Ext. 2,4-D ____________ _ _ 2,4,5-TP(Stlvex) I-chlordane -. be'ptach.lor _ hexachloroben.zene _____ _ ' hexachlorobuta.diene endrin = ~:~::ychlor ============= I -toxaphene _____ _ I _Le' PCB 5 <tJ,O"Olffm._ FOR LAB USE ONLY I Dale Received ?-/L/-C/J?'Vf 'tJJl-~eJ3s Y-17-ffVp' I Dale Extracled 8~A K-n~<JflB/'1-=-YII 8;J/f8·/1-'tlf/3& · - Date Ana.!yzedPCBs d'--/9 7'5'Yp I Reported By 1 Date Reported Lab Number I DHS 3191 (Revised l:.'93) 98ZS83 Par:unetcr Resu!ts(mg/l)(mg/kg) antimony - - arseruc barium beryllium cadmium chloride chromium cobalt copper fluoride iron lead manganese ______ _ mercury nickel nitrate selenium silver sulfates thallium vanadium zinc pH conductivity ______ _ TDS flash point ______ _ TCLP Compounds Inorganic Compounds arsenic -barium -cadmium -chromium -lead - -mercury selenium -silver - Organic Compounds benzene ca.rbcn tetrachloride -chlordane Results(mg/1) Results(mg/1) --·-·· -·-· chlorobenzene -chloroform -o-cresol m-cresol - -p-cresol cresol - -1,4-dichlorobenzene 1,2-dichloroethane - -1, 1-dichloroethylene -2, 4-dichloroethylene -heptachlor hexachlorobenzene -hexachlorobutadiene -~ hexachloroethane - -metbyl ethyl ketone n.itroben.zene - -pentachlorophenol -pyridine -tetrachloroeth y lene -trichloroethylene -2, 4,5-trichlorophenol - -2, 4, 6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Silvex) i"C _o,;,,,,rtmcnt of Environment, SAivIPLE Ai'IALYSIS REQUEST St.ate Laboratory of Public Health H~.'•.h, & Narural Rc.i;ourccli P.O. Box 28047, 306 N. Wilmington St. Solid Wu~ Mlnagcmcnt Divi,ion Ralci~h_, North Carolina 27611~8047 lite Number ftltv Oo / {p Q (o ::? s:::n SampldD C0·013·6W 08/12/98 1715 GRAB /1 _ _j_ D ::"!: . 12345678 CD081098, NC D. WILSON l'lameofSite ~iteLo~tion ~.t/ Sfl'Y ; __ C(,( tr/ ,✓;.{£ ,Collected] V '/ U/C{(, /I)(,_ DateColle< 41 If\ .fl ~ ORG-CLP EXT /PCB Ground Water ------------------ Hazardous Waste Solid Waste ~fund TCLP Compounds Sample Type I Environment.al Concentr.ite J . Ground Water (1) Solid (5) L Surface Water (2) Liquid (6) r-Soil (3) ,, Sludge (7) - Other (4);:; --Other (8) I Organic Chemistry I Parameter Results (mg/I) ~-'-'-~T:GC/MS Ac1d:B/N Ext. I_:_::_ 2,4-D. 2.4,5-TP(Silvex) -------------- chlordane - II= beptachlor hexachloroben.zene hexacPJo~obutadiene - 11= endrin : 't lindone ,. ·· '• methoxy,chlor - -toxaphene I _J.C I_ e. L. 13. s ....:o. 000 'f1k'l -p-- I . FOR LAB USE ONL y ~-1s1-rr* 'wG Date Received PCIJf ~-17-111' I Date Extracted ~,a&-11--9 ~~~ 'llfl-,i-91'13 · Date Analy~/9::'l?tf' I Reported By Date Reported ., I Ltb Number 98Z5Si\ I DHS 3 l 91 (Rtviscd 12/93) Comments Inorganic Chemistry Paro.meter Results(mg/l)(mg/kg) -antimony arsenic -barium -- -beryllium cadmium -chloride -chromium -cobalt - -copper fluoride--iron -lead - -manganese -mercury nickel -nitrate -selenium -silver -Sulfates -thallium -vanadium -zinc - -pH -conductivity TDS - -flash point - - - - - - Inorganic Compounds arseruc - - - - - - - barium cadmium chromium lead me rcury selenium silver Organic Compounds benzene -carbon tetr.ichloride -chlordane Results(mg/1) Results(mg/1) -. -···-·-·-·-·····---··-.. , ...... chlorobenune - chloroform -o-cresol -m-cresol - -p-cresol cresol - -1 .4-dichlorobenzene 1,2-dichloroethane - -1, 1-dichloroethylene -2 ,4-dichloroetbylene -heptachlor hexachlorobenzene -hexachlorobutadiene - ~ hexachloroethane - -methyl ethyl ketone nitrobenzene - -pentachloropbenol -pyridine -tetrachloroethylene -trichloroethylene -2, 4,5-trichlorophenol -2, 4, 6-trichlorophcnol -vinyl chloride endrin -lindane - -methoxychlor -toxaphe□e -2,4-D -2,4,5-TP (Silvex) I I !'lC DfP,,rtment of Environment, HCA.\1.h, & Nawral RC!;ourccs Solid Wut.e Management Divi,ion SAJ'vll'LE Ai'l'ALYSIS REQUEST St.ate Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. lsite Number Name of Site ISiteLoc:ition /ll;v Oo L fe v lo 2 -en Sample!DNuml Cr(sfl'y .Dcu tr) ,s;fc _Collected By_ Raleigh, North Carolina 276 l l-SO,n CD-019-GW 08/13/98 1020 GRAB 12345678 CD081098, NC D. WILSON UPGRADIENT FROM LAGOON ORG-CLP EXT /PCB Ground Water 121 V x'. &«I; /IJ. (__ DateCollected .Agency: --Hazardous W a.ste --Solid Waste ~fund TCLP Compounds Sample Type Inorganic Compounds Results(mg/1) I E6vironment.1I Concentrate Comments -arsea.ic { Ground Water (1) -barium Sclid (5) cadmium --L -chromium Surface Water (2) Liquid (6) le:id --- -mercury .-Soil (3) s' Sludge (7) -selenium -.... ,. silver - -Other ( 4 );$" -Other (8) - It - -. Organic Chemistry Inorganic Chemistry - 11 Parameter Results (mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) ' , ~::~/~~=(. --antimony -benzene arseruc carbon tetrachloride -- I ,_, 2.4-D ·" --·-barium -··-·--·-chlordane ---··--... --·----·-·-·-·-·-·-·····-·-·-- -2,4,5-TP(Silvex) -beryllium -chlorobenzene chlordane, cadmium chloroform ---I heptachlor chloride o-cresol I= --hexachlorobeazene -chromium m-cresol -bexachlorobutadiene cobalt p-cres~l -,, t --endrin copper cresol 11 -- lindane, r: -fluoride -1,4-dichlorobenzene methoxVChlor iron 1,2--<lichloroethane •t, .. , --toxaphene lead I, 1-dichloroethylene --11~ B.C.B. :; <o.ooo/fP!2l -m:inganese -2, 4-dichloroelhylene ;-mercury heptachlor --nickel hexachlorobenzene --- I --nitrate hexachlorobu~diene -selenium ~ hexachloroetbane --silver methyl ethyl ketone --FOR LAB USE ONLY sulfates nitroben.zene -I Date Received - 8'-/t/-9.YVf.'l/6 -thallium pentachlorophenol - -vanadium pyridine -l7etJJ ~-17-fi'VP -z.i.nc tetrachloroeth y I ene -I Date ExtractedMA f-L1-f/;~ /::Ll1 -pH -trichloroethylt!ne .tJpf1-g-, :r f · 1 · -conductivity -2, 4,5-trichlorophenol Date Analyzed /Je,85 8'-/rj-931/P -TDS . 2, 4 ,6-trichlorophenol -I Reported By . -tla.sh point -vinyl chloride --endrin lindane --Date Reported --methoxychlor I Lab Number 98ZS8S --toxaphene 2,4-D -- --2,4,5-TP (Silvcx) I DHS 3191 {Rt!vised 1:2/93) ·!'4C Dt:p,.,rtmcnt of Envii--onmcnt, Hu\th, & Narural Resources SMIPLE Ai'IALYSIS REQUEST St.ate Laboratory of Public Hes.Ith P.O. Box: 28047, 306 N. Wilmington St. Solid Waste Management Divi,ion Ra!ciyh_. North Carolina 27611-8047 lsiteNumber /ltv Ov I Name of Site ISiteLoc:ition Cr[sfl'v () y~,-J (p V (o ({ i:;-n Sample ID Numl J)ru tn 5;/c, _Collected By_ CD-019-SW 08/13/98 1530 GRAB 12345678 CD081098, NC D, W!LSOH DOWNGRADIENT FROM WETLAND ORG-CLP EXT /PCB Surface Water Date Collected 128 ' - .Agency: / ~fund --Hazardous Waste --Solid Waste TCLP Compounds Sample Type Inorganic Compounds Results(mg/1) I Environmental Concentrate Comments· -arsenic barium -uround Water(!) Solid (5) cadmium -- -chromium urface Water (2) Liquid (6) lead -- -mercury .-Soil (3) ,,, Sludge (7) -selenium - . J -silver -Other (4)l -Other (8) - II . - -Organic Chemistry Inorganic Chemistry . - I . Parameter Results (mg/I) Parameter Results(mg/l)(mg/kg) Organic Comµounds Results(mg/1) v2T:GC/MS antimony benzene --_-_ id:B/N Ext. -arsenic -carbon tetrachloride ''--2,4-D ·-barium chlordane ---·-----·-·--------··-···-·-·---···-·--·-··-·· ·-·-·---····-·-·--·-· -2,4,5-TP(Silvex) -beryllium -chlorobenzene chiordane. cadmium chloroform ---p-heptachl_o_r. -chloride -o-cresol hexachlorobenzene chromium -m:-cresol ,-- hexachlq~~butadiene cobalt p-cresol ---e:1drin copper cresol 11 ',•··· --lindane ;J fluoride l ,4-dichlorobenzene --methoxychlor -iron -1,2-dichloroethane .,. -toxaphene lead 1, 1-dichloroethylene -- I _IL:" e_c B. :i <o . Coo ft?p.n1. -manganese -2, 4-dichloroethylene --mercury -heptachlor nickel hexachlorobenzene ·--- I --nitrate -hexachlorobutadiene selenium ~ hexachloroethane -- -silver -methyl ethyl ketone FOR LAB USE ONLY sulfates nitroben.zene 0 Date Received ?-l4-9'1'J<& w G -- -thallium pentachlorophenol --vanadium pyridine -zinc tetrachloroeth y Jene . f'{!Bs F-/7-J/1' · --n Date Extracted~ )i'-L1-2Y8~2 ~ -pH -trichloror:thylene ,nr-,?-9 '8 · -conductivity -2, 4,5-trichlorophenol Date Analyzed ,8:B;5:: 3-/9-'1:?vP -TDS 2, 4 ,6-trichlorophenol -n Reported By -flash point -vinyl chloride --endrin lindane --Date Reported --methoxychlor D L,b Number 982586 --toxaphene 2,4-D -- --2,4,5-TP (Silvex) D OHS 3191 (Rcvi5cd 12/93) I I I NC J?cpa.-:mcnt of Environment, Heal!Zl, & Nawral Resources Solid Wute Management Division SMil'LE Al~ALYSIS REQUEST State Laborat.ory of Public Health P.O. Box 28047, 306 N. Wilmington St. Rateii,;h, North Cuolina 27611-8047 liteNumber filtv Oo I &vfo ~s=n Sample!DI rameofSite l 1,(sf17y ,Dcu tr] ,-5;,i .CollectedE Site Loc:ition __,{)"-----""'/_,6i---'-'-LC,..,_(.i.,_~_-. .__..,_(/;-'-'--=(__"'-----Date Callee CD-020-GW 08/13/98 0935 GRAB 12345678 CD081098, NC D. WILSON 0RG-CLP EXT/PCB Ground Water 62 .gency: Hauirdous Waste Solid Waste ~fund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) I EBvironmental Concentrate Commenti;; -arsenic / Ground Water (1) -barium Solid (5) -cadmium r -· -chromium Surface Water (2) Liquid (6) -lead - -mercury I-Soil (3) .. Sludge (7) -selenium -silver Other (4)'j; - --Other (8) - l . - -Organic Chemistry Inorganic Chemistry .. - IPararneter ' Results (mg/I) Parameter Resul ts(mg/l)(mg/kg) Organic Compounds Results(mg/1) . :. v?c;T:GC/MS -antimony -benzene ' Acid:B/N Ext. arseruc carbon tetrachloride --I 2,4-D , ; .. barium -·-·-·-·--·-·-· -· ---•-·-·-·-· -·---· chlordane -----------------· -· 2,4,5-TP,(Silvex) -beryllium -chlorobenzene chlordan1c cadmium .chloroform --- I heptachlor -chloride -o-cresol hexachlorobenzene -chromium -rn-cresol bexachlofobut.adiene cobalt p-cresol -endrin · ;,;· -- I -copper -cresol lindane i: -fluoride -1,4-dichlorobenzene methoxy,cli.lor iron 1,2-<lichloroethane ---toxaphene -lead -l, 1-dichloroethykne l_k: e1:. s. :i -<:0,0001 ,...,_ -manganese -2, 4-dichl oroeth y lene ., mercury heptachlor --nickel hexachlorobenzene ---11--nitrate -hexachlo ro but.ad iene selenium ~ hexachlor0etbane --silver methyl ethyl ketone --FOR LAB USE ONLY sulfates nitrobenzene .Date Received ';J'-/Lj-,'7?jll]J/JG -- -thallium pentachloropbenol -vanadium pyridine --l'ee5 'il-J7-'IYV/J -ZlilC tetrachloroeth y Jene -.Date Extracted /lJ.!/f f.•l?-'i..l'~~/Cm -pH -trichloroethy lene Mlff-;J74ll t0 . -conductivity -2, 4,5-trichlorophenol Date Analyzed Pc.es y-/'1-'17-VP -TDS 2, 4 ,6-trichlorophenol -I Reported By · -flash point -vinyl chloride --endrin lindane -- 1 Date Reported --melhoxychlor 982587. --toxapheae Lab Number 2,4-D -- --2,4.5-TP (Silvex) DHS 3191 (Revised J:/93) I I: ~C Dql,.-:tment of Environm~nt, Hc.&!'11, & N1.wral Resources SAlvIPLE Ai~ALYSIS REQUEST Slate Ubomory of Public Health P.'O. Box 28047, 306 N. Wilmington St. Solid Wut.e !'A•naicmcnt Divi,ion Raleii;h.' Nonh Carolina 27611-8047 . lsiteNumber /vtv Oo / [p '{) (o :? s=n Sample!DNuo CD-024-SW 08/10/98 1S20 GRAB "I'-12345678 CD081098, NC D. WILSON Name of Site C,(sfl'y ,Dcu 1n Si:;. ,Collected By-' ORG-CLP EXT/PCB Surface Water ISiteLoc:itio□ ~t)~'/~·fr:~J r,_.~_,~'-l---~/IJ~'~(__~ ___ DateCollected ____ ---;:::=====----7-8 ___ _::....., .Agency: __ Hazardous Wa.ste __ Solid Waste ~fund Sample Type I Environmental tround Water (I) ~ Surface Water (2) Soil (3) :.. Other (4).'., Concentrate -Solid (5) -Liquid (6) -Sludge (7) -Other (8) It Organic Chemistry ,,: Parameter ., 1 _ P9'T:GC/MS _,,_ '_!Acid:BiN Ext. r,, 11= 2,4-D ,, 2,4,5-TP(Silvex) chlordane Results (mg/I) 11 -bepLlchJor hexachlorobenze:::ie --hexachlorobut.1diene _____ _ e:idrin ·:, lindane ·t methoxychlor 11 _ toxapherie I .JL_ PCS $ I=-. __ __, FOR LAB USE ONLY n Date Received <j'-/ 'I -'f?Vt_ul6 ,PCl!JS-Y-17-9:J'YP D Date Extracted /3,.)I} 'l-/ 1·9'1BiJ.:::r;,, /Uh Mlrf'-13-'lit/l) 1 . Date Analyzed IPc.is: 1?-/9-'l?VP E Reported By Date Reported _________ _ m Lab Number 982S88 II DHS 3 ! 91 (Revised 12/93) Comments Inorganic Chemistry Parameter Results(mg/l)(mg/kg) - - antimony. arsenic barium beryllium cadmium chloride chromium cobalt copper fluoride iron lead _,, ____ _ manganese ______ _ mercury nickel nitrate selenium silver sulfates thallium vanadium zinc pH conductivity ______ _ TDS flash point TCLP Compounds Inorganic Compounds Result.s(mg/1) arseruc -barium -cadmium -chromium -!C'1d - -mercury selenium -silver - Organic Compounds Rcsults(mg/1) benzene -carbon tetrachloride -chlordane -· chlorobenzene -chloroform -o-cresol -m-cresol - -p-cresol cresal - -1,4-dichlorobenzene -1 ,2-dichloroethane -1, 1-dichloroethyle□e -2, 4-dichloroethylene -bepLlchlor hexachlorobenzene -hexachlorobutadiene -... hexachloroethane -_ methyl ethyl ketone nitroben.zene - -pentachlorophenol -pyridine -tetrachloroethylene -trichloroethy lene -2,4,5-trichlorophenol -2,4, 6-trichlorophenol -vinyl chloride endrin - lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Si\vex) 1 · . NC Dcpo,tm,nt of Environm,nt, SMIPLE Ai'l"ALYSIS REQUEST St.ate Laboratory of Public Health Hultil,-& Naoual Ruourccs P.O. Box 18047, 306 N. Wilmin!,>1on St. Solid Wutc Management Divi,ion Rali:.ii,:h_, North Carolina 27611~8047 lite Number f/tv Ov / &, l) lo 4 s=n Sample ID Nur C0-025-SW 08/10/98 1615 GRAB _j_ 12345678 CD081098, NC O. WILSON ( 1r(Sfl'Y ,Dcu fr7 ,.s;:/4: ,Collected By_ ,,ameofSite Siteloc.:ition .Agency: .1} / ORG-CLP EXT /PCB Surface Water () '/ f77;,-4? /IJ (__ DateCollected: ~---===::..:._· --==8=5====::...., ~fund TCLP Compounds Ha=dous Waste Solid Waste Sample Type I Environmental Concentrate Ground Water (1) 12 Surface Water (2) t-Soil (3) ,,• Other (4) ,'• - - - - Solid (5) Liquid (6) Sludge (7) Other (8) Comments l-----,---- Organic Chemistry Inorganic Chemistry :,, !Parameter · . _ P§:T:GC/MS . _VAcid:B/N Ext. ''·I I 2 4-D ,, :::.=_ 2:4,5-TP(Silvex) II= chlordane bepLllchlor hexachloroben.zene Results (mg/I) ------ -hexachlq~obutadiene~----- I endrin -lindane ,, = methoxy_;_hlor I _ toxapht!ne ..L<: PCR s <t>, ""o!tpm- - -1----- I . FOR LAB USE ONLY. Date Received <,?-/t/-1';/V/J, 'tJk; lf'(,l!Ji 'lf-/7-?3'9P I Date Extracted 1'!4:ffi.I/ f'.!!jh~ t:./h ~-/ S'-•'l!f< . Date Analyzed f'C/3~ 8-/'J-9fn/P I Reported By 1 Date Reported Lab Number I DHS 319! (Revi~cd 12/93) 982589 Parameter Results(mg/l)(mg/kg) ,- antimony arseruc barium beryllium cadmium chloride ~hromiUrn cobalt copper fluoride iron lead ----·--·--··· manganese ______ _ mercury nickel nitrate selenium silver sulfates thallium vanadium zinc pH conductivity ______ _ TDS flash point ______ _ Inorganic Compounds Result.s(mg/1) arsenic -barium -cadmium -chromium -lead - -mercury selea.ium . -silver - - - - Organic Compounds Result.s(mg/1) benzene -carbon tetrachloride -chlordane --·-ch.!orobenzene - Chloroform -o-cresol -m-cresol - -p-cresol cresol - -1,4-dichlorobenzene 1,2-dichloroethane - -l, 1-dichloroethylene -2, 4-dichloroethy lene -heptachlor hexachlorobenzene -hexachlorobutadiene -... hexachloroethane -_ methyl ethyl ketone nitrobenzene - -pent.achlorophenol -pyridine -tetrachloroeth y lene -trichloroethylene -2, 4,5-trichlorophenol -2, 4 ,6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphene -2,4-D -2,4,5-TP (Silvex) 1 · . ?:"C DC'pa~mcnt of Environment, • Hcal1!1, & Nawral RC1>ources Solid Wute Muugcmcnt Divi,ion SAfvIPLE Ai~AL YSIS REQUEST State LaboralOry of Public Health P.O. Box 18047,.306 N. Wilmington St. Rald~h. North Carolina 27611-8047 lite Number ftltv OD / /p D (o ::? :>=n Sample ID Numb, C0-026-SW 08/10/98 1615 GRAB ( . /ameofSite Cr(sfl'y ,Dcu Ir'/ ,s;± ,Collected By_ 12345678 C0081098, NC 0. WILSON If\ .fl .J ORG·CLP EXT/PCB Surface Water iteLoc:ition~V~~K~t~V~o .. ~ .. 7-· +--~(l)~_C--~ ____ DateCollected 92 tgency: --Hazardous Waste --Solid Waste ~fund TCLP Compounds Sample Type Inorganic Compounds Results(mg/1) I Environmental Concentr.ite Comments -arsenic barium - ~round Water (1) Solid (5) cadmium --~ Surface Water (2) -chromium Liquid (6) -lead - -mercury 1-Soil (3) Sludge (7) selenium :, --,. -silver Other (4)<;,' Other (8) --- I - ' -Organic Chemistry Inorganic Chemistry - 'Parameter Results (mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) ~T:GC/MS antimony benzene -' . = td:B/N Ext. -- -arseruc -carbon tetrachlorid~ ,~--2,4-D , barium chlordane 2,4,5-TI'(Silvex) ·-----------·---··-·-· ---·-· ·---····· -----· ------· ·---·--·--·-.. ---·· -beryllium -chJoroben.zene chlordane cadmium chJorofonn ---- l heptachlor -chloride -o-cresol hexachlorobenzene -chroiruurn -m-cresol hexachlo!pbutadiene cobalt p-cresol --- I endrin ·::-copper cresol --lindane ._• fluoride 1,4-dichlorobenzene --methoxychlor . iron 1,2-dichloroethane .,. --toxaphene -lead -1, 1-dichloroethylene 1~ e_c. B. :i < o, o o o I fJ/2LlL -manganese -2, 4-d i ch 1 oroethy Jene I mercury heptachlor --nickel · hexachlorobenzene ---l--nitrate -bexachlorobutadiene selenium ~ hexachloroetbane --silver methyl ethyl ketone --FOR LAB USE ONLY -sulfates nitroben.zene D Date Recei ve<l - -thallium pentachloropbenol Y-Lt./-CJ 8'VJ!?:W6 - -vanadium pyridine -f'eB;. r-17-W -zinc tetrachloroethylene -·uDate Extracted A/Jd s,'.-n-2~.::m i;m -pH -trichloroethylene l).(),ff-lf-'/8' !.() J . -conductivity -2, 4,5-trichlorophenol Date Analyzed tfrR's 3-/9-9'i?'{P -TDS 2, 4 ,6-trichlorophenol -- .Reported By -flash point -vinyl chloride --endrin ' --lindane Date Reported --methoxychlor ILab Number u.; , ....... ,_-- ---toxaphene ''982590 2,4-D -- -2,4,5-TP (Silvex) I OHS 3191 (Revised 12/9)) I ?:-IC Department oi Environment, Hu!.:li, & Narural Ruourccs SAl\tlPLE Al'IALYSIS REQUEST State LaboralOry of Public Health P.O. Box 28047, 306 N. Wilmington St. Solid Wut.e Management Division lite Number ftl'tv Oo I fe V lo ;:; s=n Sample ID Number, 1/ameofSite Cr(sf17y ,Dcu h1 'S:± _Collecte<lBy __ l SiteLoc:ition ~V~i~&~i~G--u.,_~----,· ·-~/IJ~l-~ ___ Date Collected .gency: Ha=dous Waste Solid Waste ~fund ---- Sample Type I Environmental Concentrate Comments j Ground Water (I) -Solid (5) I_ Surface Water (2) -Liquid (6) .-Soil (3) . : . -Sludge (7) Other (4);' Other (8) -- II . Organic Chemistry Inorganic Chemistry Ra.l!!il:h_, North C1rolina 27611-8047 CD-028-GW 08/12/98 1205 GRAB 12345678 CD081098, NC D. WILSON PERMANENT HON!TORING WELL ORG-CLP EXT/PCB Ground Water 132 TCLP Compounds Inorganic Compounds Result.s(mg/1) arsenic -barium -cadmium -chromium -lead - -mercury selenium -silver - - - - -I Parameter Results (mg/\) Parameter R esul Ls (mg/I) (mg/kg) Organic Compounds Result.s(mg/1) ~T:GC/MS antimcny benzene --_ 1d:B/N Ext. arseruc -carboll tetrachloride --I 2,4-D , . barium chlordane ·--· 2,4,5,TP(Silvex) ------·-·---.. ---··. ··-·---·-·-·--· ____ ., __ , . -·--· ·-·-. --·-·· -·-·---·--. -·-· - -beryllium --chloroben.zene -' -chlord~~ -cadmium -chloroform heptachlo_r chloride o-cresol I= --hexachloroben.zene chromium m-cresol --hexachl0robutadiene cobalt p-cresi;,I -.,/ -- 11 endrin 1 ··, -copper -cresol lind.1.ne·,{_: -fluoride 1,4-dichlorobenzene - methoxxchlor iron 1,2-dichloroethane ---toxaoherle -lead I, 1-dich!oroethylene II~ £ L. 8. -s <11,0/JI}~ -manganese -2, 4-dichloroethylene -mercury -heptachlor nickel bexachlorobenzene --- I -nitrate hexachlorobutadiene --seknium ~ bexachloroethane --silver methyl ethyl ketone --FOR LAB USE ONLY sulfates nitrobenzene I Date Received tJ?-/~ -9:{~hJ& -- -thallium penUJ.chlorophenol -vanadium. pyridine -- ZlnC tetrachloroeth ylcne PaB.fY-/7-VP --I Date Extracted e~-11 -'i'~B~-):ft\ -pH -trichloroethylene ~ -,r-'i-YRJ ' . -conductivity -2, 4,5-trichlorophenol Date Analyzed R:Br 1[-1'7--'l?W' -TDS 2,4 ,6-trichlorophenol -I Reporte<l By -flash point -vinyl chloride --endrin lindane --Date Reporte<l --methoxychlor I L:ib Number 982591 --toxaphene ' 2,4-D -- --2,4,5-TP (Silvex) I DHS 3191 (Revi.mj 12/93) ' ' 1· ~C Dqiu:mcnt of En ... ironment, He.al:l1, & Natural Resources SAiv!PLE Ai'l'ALYSIS REQUEST St.ate Laboratory of Public He.ah.h P.O. Box 28047, 306 N. Wilmington St. Solid Wule Mani.gcmcnt Divi,ion Rali:iyh .• North C.uolina 27611-8047 liteNumber /vt;v OD I (p D(o c2 'LO Sample!DNuri C0-029-GW 08/12/98 1510 GRAB · 12345678 C0081098, NC 0. WILSON i/:uneofSite ~iteLoc:ition Cr(sff'v v vfv!,~ 1i)ru fn ,5~,i ,Collected By_; PERMANENT HOHITORIHG WELL " ~ ORG-CLP EXT/PCB Ground Water · /IJ l---Date Collected 136 - .gency: H=u-dous W a.ste Solid Waste ~fund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) I Jnvironmental Concentrate Comments -arsenic barium -Ground Water (I) Solid (5) cadmium .--- -chromium Surface Water (2) -Liquid (6) -le;id -mercury t-Soi! (3) , '.. -Sludge (7) -selenium . ' silver " - -Other (4}•. -Other (8) -r Org~nic Chemistry - -Inorganic Chemistry - IParameter Results (mg/I) Par:-imeter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS antimony benzene -~id:B/N Ext. --arsenic carbon tetrachloride 1---i --2,4-n _ .. __ barium ., --·----··--··· ·-· ··-·-·-· ··-chlordane ·---...• ----------·---·--···-· 2,4,5-TP(Silvex) -beryllium -chlorobenzene chlordaoe cadmium chloroform --- I heptachlor -chloride o-cresol - hexachloroben.zene chromium m-cresol -- hexachlorobutadienc cobalt p-cresol -... , --endrin ,, copper cresol I= ,, --lindane ·, fluoride 1,4-dichlorobenzene ' --- rnethoxychlor iron 1,2-dichloroethane ---toxaphene lead I, 1-dichloroethy Jene 1_0 --e.t:. 8. ::i < o. ooo I ff-"'--manganese -2, 4-d i chloroeth y Jene -mercury -beptachlor nickel hexachloroben.zene ---t--nitrate bexachlorobutadiene -selenium ~ hexachloroethane ---silver methyl ethyl ketooe • --FOR LAB USE 0:S.'L Y sulfates nitrobenzene I Date Received 'F-/{J-'z~ W£ --thallium pentachlorophenol -- -vanadium pyridine -z.inc tetrachloroethylene Pees Y-t7-P ---I Date Extracted 'IJ1-e.-a-'i.~BIP,:rfJkKL}:1 -pH -trichloroethylene lrff"1-f-9f8 -conductivity -2 ,4,5-trichlorophenol Date AnalyzedP@ F--/'l-z'YVP TDS 2, 4,6-trichlorophenol --I Reported By -flash point -vinyl chloride --endrin lindane -- 1 Date Reported --methoxychlor 982592 --toxaphene Lab Number 2,4-D -- --2,4,5-TP (Silvex) DHS 3191 (Revised 1::93) j I I NC Depu~mcnt of Environment, Healt.'1, & N1rural Resources SMIPLE A.t'IALYSIS REQUEST St.ate Laboratory of Public Health P.O. Box ::!8047, 306 N. Wilmington St. Solid Wu~ Man1gemcnt Divi,ion liteNumber Jltv Oo I /p V (o ,;; s:=n Sample ID N umbe, C0-030-GW , · · 12345678 l'lameofSite ~iteLoc.1tion Cr(sft"v e {fr,,~ 1Dcu m < Si le _Collected By __ ~ I /' ORG-CLP IV t----DateCollectul -- .geocy: Hazardous Waste Solid Waste ~fund ---- • Sample Type I Environmental Concentrate Comments / Ground Water (I) -Solid (5) L Surface Water ('.'-) -Liquid (6) .-Soil (3) ,., '. -Sludge (7) :• Other (4);\ -·-Other (8) t •\ Organic Chemistry Inorganic Chemistry IParameter Results (mg/I) Parameter Results(mg/1) (mg/kg) P&T:GC/MS -antimony ' -i/4id:B/N Ext. ·arseruc - I -- 2,4-D 4, barium -----··· --·-·-·-·-··--·--·--·-·- 2,4,5-TP(Siivex) -be,ylliurn -chlordm~ -c:idrnium I= hept.1chlor -chloride hexachloroben.zene chromium - hexachlorobutadiene cobalt -endrin · ·~:. - I -copper lindane ~i" -fluoride methoxychlor iron -,,. . -toxaphene -lead 1-.k: £Cc8 :i <o. OOO'lJf2-/>\ --manganese mercur; - nickel --1:-nitrate -selenium -silver -FOR LAB USE ONLY sulfates .Date Received 8'-/L/ ~ lf1J$WA - -thallium -vanadium zinc fetJS ?-lr'-93' -I Date Extracted .&)/11 -11-'lm~rz, µn -pH fr)l'r~-ll'-9 ~ . -conductivity Date Analyzed P<;,Bf 'iJ-.:U, -9?VP -TDS I Reported By . -flash point - -Date Reoorted .Lab Nu~ber - 982593 - - I DHS 3191 (Rt:Vi5t:d 12/93) - Ralcii::h_, North Carolina 27611-80,n 08/11/98 1705 GRAB CD081098, NC D. WILSON EXT/PCB Ground Water 103 TCLP Compounds Inorganic Compounds Results(mg/1) arsenic -barium -cadmium -chromium -le:id - -mercury selenium -silver - - - - - Organic Compounds Re:sults(mg/1) benzene -carbon tetrachloricie -chlordane ---·· _____ ,. __ -. ----- chlorobenzene -chloroform -o-cresol -m-cresol - -p-cresol cresol - -1,4-dichlorobenze□e 1,2-dichloroethane - -1, 1-dichloroethylene • -2, 4-dichloroethylene -heptachlor bexachlorobenzene -hexachlorobutadiene - ~ hexachloroetbane - -methyl ethyl ketone nitrobenzene - -penLachlorophenol -pyridine -tetrachloroethylene -trich.l oroeth y lene -2, 4 ,5-trichlorophenol -2, 4 ,6-trichlorophenol -vinyl chloride endrin -lindarie - -methoxychlor -toxaphene -2,4-D -2,4,5-TP (Silvex) -- I' NC Dc_panmcnt of Environment, Hu.Ith,&. Narural Rc.&ourcc& SM1PLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Ra!d1,:h, North Carolina 27611-8047 l Solid Wut.e Management Divi,ion iteNumber ft!Cv Oo I ,,ameofSite Cr/sfl'y {; V lo ::? 7-;'[) Sample!DNuml ' J)r11 tr) ,5;fc ,Collected By_ C0-031-GW 08/11/98 1850 GRAB 12345678 CD081098, NC D. WILSON SiteLoc;ition _~t)~-K~~fv~~G_i;:;.,,~~• ;---~/1)~-~L--~ ______ Date Collected ~gency: __ Hazardous Waste __ Solid Waste ~fund ORG-CLP I Sample Type EqVironmental Concentr.lte f Ground Water (I) _ Solid (5) _ Surface Water (2) _ Liquid (6) I-Soil (3): Other (4)• Sludge (7) Other (8) Comments 11~-----,----- Organic Chemistry Inorganic Chemistry f' 'Parameter •,1 _ P§:T:GC/MS r,·,~.~~~B/N Ext. __ 2,4,5-TP(Silvex) chlordane Results (mg/I) ' heptachlor hexachl6robenzene ------hexachl9fobutadiene _____ _ ~-~:~::;Liar Parameter Results(mg/l)(mg/kg) antimony arseruc barillm beryllium cadmium chloride chromium cobalt copper fluoride iron lead ---·-·---------·-- I _ toxaphene ~ PCB s <o.ooo/f?i"-'" ·-manganese ______ _ - 1= I FOR LAB USE ONL y . Date Received ?-/l/-9J'~µJG, d'C/Ji 'lT-lo-'lT ~ I Date Extracted~~9'-/1-,'~,~ <;'-/ J'-9 li'/3 . . Date Analyzed ftB_; 1:-.::/0-'(/?VP I Reported By I Date Reported Lab Number I OHS lt9! (Revised t2/9J) 982594 - - - - - - -- - - - - - - - - - - - mercury · nickel nitrate selenium silver sulfates thallium vanadium zinc pH conductivity TDS flash point EXT/PCB Ground Water 107 TCLP Compounds Inorganic Compounds Results(mg/1) arseruc -barium - cadmium -chromium -lead - -mercury selenium -silver - Organic Compounds Results(mg/1) benzene -carbon tetrachloride -chJordane ---chlorobenzene -chloroform -o•cresol -m-cresol - -p-cresol cresol - -1,4-dichloroben.zene 1,2-dichloroethB.Tie - -I, 1-dichloroethylene -2, 4-dichloroetbylene -heptachlor hexachlorobenzene -hexachlorobutadiene -... bexachloroetba.ne -_ methyl ethyl ketone nitrobenzene - -pentachloropbenol -pyridine -tetrachloroethylene -trichloroethylene -2, 4, 5-t rich! orophenol -2, 4 ,6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Silvex) I ~C Dqu.:1mcnt of Environment, Health,&. Narural Ruources . Solid Wut.c Muagcmcnt Division liteNumber /vi)) Oo I ( ameofSite iteLoCJ.tion C,(sfl'v SAivll'LE Ai','ALYSIS REQUEST SL.ate Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Raldi,:h, Non.h C1.rohna 27611-&047 fR 1) (o ,;; '2°0 Sample ID Nw CD-032-PW 08/13/98 1308 GRAB 12345678 CD081098, NC D. WILSON [)cu tr) ,..S:4: _Collected By. POTABLE WELL OR6-CLP EXT/PCB Ground Water /iJ L--DateCallecteL ___ _ 111 Vttvc~ - .ge□cy: Hazardous Wa.ste Solid Waste ~fund TCLP Compounds -- -- Sample Type Inorganic Compounds Results(mg/1) I Environmental Concentrate Comments -arseruc ✓Ground Water (1) barium - Solid (5) cadmium -- L chromiuIIl - Surface Water (2) Liquid (6) -lead --mercury r-Soil (3) • Sludge (7) -selenium - -silver Other (4) :-Other (8) --- t - - Organic Chemistry Inorganic Chemistry - I Parameter • Results (mg/I) P::ira.meter Resui'ts(mg/1) (mg/kg) Organic Compounds Resu!ts(mg/1) ~T:GC/MS -antimony -benzene 1 = id: BIN Ext. -arsenic -carbon tetrachloride _ 2,4-D . . barium chlordane . ----------·----·-··---· ------· .. -·-·--·-·-·-· ·---· ·------•· 2,4,5-TP(Silvex) beryllium chlorobenzene -.. --chl0roform chlordane cadmium --- II= heptachlor -chloride -o-cresol hexachlorobenzene chromium -m-cresol - hexachlorobutadiene cobalt p-cresol -y. -- 11= endrin · •/•\ copper -cresol -lindane ;J; -fluoride -1,4-dichlorobenz.ene ,, methoxy_~hlor iron 1,2-dichloroethane --- -toxaphene -lead -l, 1-dichJoroethylene I _k: /:.CB. :, < O. QOO ~I!/!."'--manganese -2, 4-d_ichloroethy leoe --mercury -beptachlor nickel hexachlorobenzene --- I --nitrate -hexachlorobutadiene selt!nium ~ hexachloroethane -- -silver -methyl ethyl ketone FOR LAB USE ONLY -sulfates n.itrobenzene I Date Received ~-Jt/--9!}{?16 - -thallium pentachlorophenol -vanadium pyridine -- ZlnC tetrachloroethylene -Res 'i'-/3-9 'P --I Date Extracted ~li.'l.:11-'1.&',!3~r -pH -trichloroethy lene tw/f '17 K-9 B . -conductivity -2 ,4,5-trichlorophenol Date Analyzed p~:f 8:-~ 0-9?:V'P -TDS 2, 4,6-trichlorophenol -I Reported By -flash point -vinyl chloride --endrin lindane --Date Reported --methoxychlor I Lab Number 982595 --toxaphe□e 2,4-D -- --2,4,5-TP (Silvex) I DHS 3191 (R¢vised 11f93) NC Depu:mcnt of Environment, Hcallh, & Natural RCj;ourcc:s SMil'LE Ai'IALYSIS REQUEST Slate Laboratory of Public He.alth P.O. Box 28047, 306 N. Wilminbrton St. Solid Wuua Man.agemcnl Divi,ion Ralei~h_, No~ ':'..aroli.na 27611·8D•n liteNumber rev Oo· / {p 1) (o (;? s=n SamplelDNumbe C0-040-SW 08/13/98 1625 GRAB ...L • 12345678 C0081098, NC D. WILSON EXT/PCB Surface Water ( ameofSite 9:(sjl'YI rDflc/11~ ,.5;/c,eo11ecte<lBy_ ORG-CLP ~iteL.ocation ~[)~=x'.~CT.-!~C,_.,~,t-')----,· ·e--~-~~<...---~ ___ DateCollected ---;::=======--==1=4=0====-. .gency: Hazardous Waste Solid Waste ~fund Sample Type I Environmental Concentrate _ /round Water (I) If Surface w.ater (2) r-Soil (3) : Other (4\:, Solid (5) Liquid (6) Sludge (7) Other (8) Organic Chemistry Parameter _ P§ff:GC/MS ~cid:B/N Ext. 2,4-D .. 2,4,5-TP(Silvex) chlordane beptacWor hexachloroben.zene Re.suits (mg/I) ------ hexachlorobut.adiene~----~ endrin \;; lindane-'C: rnethox}'Chlor toxaphene _k:: PCB s -<:O.OO(J/ FOR LAB USE ONLY I Date Receive<l. g'°-/£/-'ffV/;o./6 pe9:r r-lY-9'?yp I Date Extracted 'jfj'i1-11-9'iff ::rlh ,F,M '/1 9'•1--j'• .f'~Jd)' . Date Analyzed PcBf 3-,;J...0-'Jfyp I Reporte<l By Date Reporte<l , I Lab Number __ 9_8_2_5_9_6 __ I DHS 3191 (Revi5ed 12/93) Comments Inorganic Chemistry Parameter Result.,(rng/l)(mg/kg) antimony arsenic barium beryllium cadmium chloride chromium cobalt copper fluoride iron lead manganese ______ _ rnercur; nickel nitrate selenium silver sulfates thallium vanadium zinc pH conductivity ______ _ TDS flash point TCLP Compounds Inorganic Compounds arsenic ba..;.um cadmium chromium lead mer:-ury selenium silver Organic Compoands benzene carbon tetrJchloride chlcrdan<' chiorobcnzene chloroform o•cresol m-cresol p·cresol cresoi l ,4·dichlorobe~ne 1,2-dichloroethane Results(mg/1) Results(rng/1) I, 1-dichJoroethylene ______ _ 2,4-dichloroethykoe ______ _ beptacWor hexachlorobenzene hexachlorobutadiene ______ _ ... hexachloroethane methyl ethyl ketone nitrobenzene: pcnt.achlorophenol py,idine tetrachloroethylene trichJoroethylene 2,4,5-tricWorophenol ______ _ 2,4,6-trichlorophenol ______ _ vinyl chloride_ endrin lindane methoxycWor toxaphene 2,4-D 2,4,5-TP (Silvex) 1. SMIPLE Ai~ALYSIS REQUEST St.ate La.boralOry of Public Health NC Dr,partmcnt of Environment, Hc.allh, & Narural Ruourccs P.O. Box 18047, 306 N. Wilmington St. I Solid Wu« Mrn.,g,m,m Divi,ion SiteNumbcr ft!Cv Oo / fevfo (<r:;-:n Sample!DNun C0-113-GW 08/12/98 1715 GRAB R.alei1:h., North C1.rolin1 27611-8047 C . _j_ :.i_ 12345678 CD081098, NC D. WILSON l'lameofSite ;(sJl'YI ;()cu /r7 ,s;([. _Collected By_ ORG-CLP EXT/PCB Ground Mater 43 SiteLoc:ition t/ '{t7f;rzi; /IJ L---DateCollected_ .Agency: __ Hazardous Waste __ Solid Waste ~fund TCLP Compounds - I Sample Type E[llVironment.al Concentrate I J Ground Water (1) _ Solid (5) _ Surface Water (2) _ Liquid (6) I- ll- Soil (3) Other (4)' Sludge (7) Other (8) Organic Chemistry i·I J.·, ,. Parameter P&T:GC/MS -i::/4id: BIN Ext. 2,4,D Results (mg/1) 1, ·1 'i:' ·1~ 2,4,5-TP(Silvex) chlordan,e heptachlor hexacl'-Joroben.zene 1.= ------hex:i.chlofobutadiene I. ------endri.n '' .. lindane _ melhoxychlor I toxaohene ..Jc' PCB s .. - 1= I FOR LAB USE ONL y ' Date Received u'l-?fg lV6 '1-tCJ~tM 4Je,1 I Date Extracted~ Y-/Y:'i'YVP 8JJA-y-7'1-i} f IJ "9 . Date Analyzed £CB,--Y--.;;?o-9NP I Reported By I Date Reported _________ _ Lab Number 982597 I DHS 3191 (R(.viscd 12/93) Comments Inorganic Chemistry Parameter Results(mg/l)(mg/kg) antimony arseruc barium -beryllium cadmium chloride chromium cobalt copper fluoride iron lead manganese mercury nickel nitrate selenium silver sulfates thallium vanadium zinc pH conductivity TDS flash point Inorganic Compounds Results(mg/1) arseruc -barium -cadmium -chromium -le:id - -ILercury selenium -silver - - - - - Organic Compounds Results(rng/1) benzene -carbon tetrachloride - chlordane -... ·-·--· -· ,.,_,._,, ____ ..... _. chlorobenz.ene -chloroform -o-cresol - rn-cresol - -p-cresol cresol - -1,4-dichlorobenzene 1,2-dichloroethane - -1, 1-dichloroethylene -2, 4-d i ch Io roe thy lone -heptachlor hexachlorobenzene -bexachlorobutadiene - ~ hexachloroetbane -methyl ethyl ketone nitrobenz.ene - -pentachlorophenol -pyridine -tetrachloroeth y l ene -trichloroethylene -2,4 ,5-trichlorophenol -2,4 ,6-trichlorophenol -vinyl chloride endrin - lindane - -methoxychlor -toxaphene ' -2,4-D -2,4,5-TP (Silvex) I .. t"C Dcpa,"tmcnt of Environment, Hr.al'lh, & Natural Resources Solid Wane Management Division SMIPLE At~ALYSIS REQUEST St&.tc LaboralOI)' of Public Health P.O. Box 18047, 306 N. Wilmington St. Ralci);h, North C.trolina 27611-8047 liteNumber ftltv Oo / ~ Q (o ~ z::;:n Sample ID Ne C0-126-SW 08/10/98 1615 GRAB 12345678 C0081098, Ne· 0. WILSON Cr[sff'y ,Dru tr/ ,.S:4:; .Collected By .Name of Site Site Location .Agency: ORG-CLP t) '/ f;;;,..-~ /IJ (__ · DateCollectec ~fund Hazardous Waste Solid Waste -- -- I Sample Type Environmental Concentrate Comments 7 round Water (1) Solid (5) -I_ Surface Water (2) Liquid (6) -,. r--Soil (3) ·.) Sludge (7) ::t -.. -Other ( 4);1 -Other (8) II Organic Chemistry Inorganic Chemistry 11 Parameter Results (mg/I) Parameter Results(mg/l)(mg/kg) ~T:GC/MS -antimony _ ,d:B/N Ext. -arsenic I 2,4-D barium ------------·-·-·-----·-··-·-·- -2,4,5-TP(Silvex) -beryllium chlordane cadmium -- II= he?tach!o·r -chloride hexachlof'obenzene -chromium hexachlorobutadiene cobalt -endrin ::~· - I!= -copper lindane :;" fluoride -methoxyshlor iron --loxaphene -lead 11-k: e. c. B :, <"•000/~ -manganese -mercury nickel -- I --nitrate selenium -silver -FOR LAB USE ONLY sulfates D Date Received J;;,1£1-'f'Mf'v/6. - -thallium -vanadium . . </--l,?J-CJ yA/Jw o, -zinc E Date Extracted tPC.l?s !T-17-~00 -pH 6#11 D'-19-rt.9& -conductivity Date Analyzed ,PC/3s g'-.;20-9?VP -TDS E Reported By -flash point - -Date Reported -I L:ib Number 982598 - - -DHS 3191 (Revised 12/93) EXT/PCB Surface Water 99 TCLP Compounds Inorganic Compounds Results(mg/1) arsenic -barium -cadmium -chromium -lead - -mercury selenium -silver - - - - - Organic Compounds Results(mg/1) benzene -carbon tetrachloride -chlordane ···-·· . ·,,. chlorobenz.ene -chloroform -o-cresol -m-cresol - -p-cresol cresol -1,4-dichlorobenzene -1,2-dichloroethane - -I, 1-dichloroethylene -2, 4-dichloroethyleoe -heptach!or hexachlorobenzene - hexachlorobutadiene - ~ hexachloroethane - -methyl ethyl ketone nitrobenzene - -pent.achlorophenol -pyridine -tetrachloroeth y lene -trichloroethy lene -2, 4,5-trichlorophenol -2, 4 ,6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphene -2,4-D -2,4,5-TP (Silvex) NC Dcpaitmcnt of Environment, He.allh, & Natllral Resources SAlvIPLE Al'IALYSIS REQUEST St.ate Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Solid wa',tc Management Diviliion R.aleii;h_, North Carolina 27611-8047 lite Number /!ft D Oo / fe V lo ::? .:;:n _Sample ID Numb CD-200-RB 08/11/98 1000 COHP _j_ Q ~ J ' 12345678 CD081098, NC D, WILSON riameofSite 9:(5Jl'YI r_fllcu:7 ,);!£, _Collected By_ ORG-CLP EXT/PEST Rinsate Si teLo□tion _,t:J"-_,,'/_·,_ty,""J'-"C,-/;;1,1-7+•-...L_.:....o<---c:.... ___ Date Collected .. 1 5 4 -- ~gency: Hazardous Waste Solid Waste ~fund TCLP Compounds ---- I Sample Type Inorganic Compounds Results(mg/1) Environment.al Concentrate Comments -arseruc barium - Ground Water (I) Solid (5) cadmium r --- -chromium Surface Water (2) Liquid (6) lead --- -mercury ~ Soil (3) ',~ Sludge (7) selenium --silver ~ther (4)< - --Other (8) - ll - -Organic Chemistry Inorganic Chemistry -I r Parameter Results (mgil) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS -antimony -benzene i::4id: BIN Ext. arsemc carbon tetrachloride I --2,4-D ----hariurn --·-·---·-· ··-··-··---· ·•---,--·-·---·. chlordane I -----·------·-·--·---·-· ---· 2,4,5-TP(Silvex) beryllium chlorobenzene ----chlordane cadmium chloroform ---a -I -heptachlor -chloride -o-cresol -hexachlorobenzene -chromium -rn-cresol -hexachlorobutadieoe -cobalt -p-cresol , .. I endrin ., copper cresol -. -lindane £~·, - fluoride 1,4-dichlorobenze□e -_., -- methoxvchlor iron 1,2-dichloroethane --,, -- I -toxaphene lead 1, 1-dichloroethyle□e --...1L" e. C. & :i -<P, ooo/~ --manganese -2, 4-dichloroethyle□e -mercury · heptachlor -- nickel hexachlorobenzene ---~ --nitrate bexachlorobutadiene -selenium ' hexachloroetbane -- -silver methyl ethyl ketone -I FOR LAB USE 'Ot<.'L y sulfates nitrobenz.ene -- -thallium pentach1orophenol - Date Received £;1'-f •o/~~$.'zb vanadium . pyridine --A-r-11 ro-:1tJoi -ZlllC tetrachloroethylene -I Date Extracted~ t,-;?-9f1tr -pH -trichloroethylene · 'l'J -1 -1115 . -conductivity -2, 4, 5-trichl orophenol Date Analyzed W'r 1/-.;l..O -"J§'W TDS 2,4 ,6-trichlorophenol --I Reported By -flash point -vinyl chloride --endrin lindane -- 1 Date Reported --methoxychlor 982599 --toxaphene Lib Number 2,4-D -- --2,4,5-TP (Silvcx) DHS 3191 (Revised 1'2/93) a r I NC D,.-par;mcnt of Environment, H~lU'l, & Natural Resource, SAL'vIPLE AL'IALYSIS REQUEST St.ate Labor:alOry of Public Health P.O. Box 28047, 306 N. Wilmington St. Solid Wut.e Management Divi,ion Raleit:h, North Carolina 27611-8047 liteNumber lvCn Oo I t V lo ,;;! s:::o Sample ID Number {)r(sf~y ,Dcu tr') \ s;:;{ µ,llectedBy_: C0-400-0B 08/14/98 1300 GRAB 12345678 C0081098, NC 0. WILSON rameofSite SiteLoC3tion l\gency: 01 BLANK ORG-CLP t) tfvC{~ /I)(__ DateCollected_ __ Solid Waste ~fund Hazardous Waste Sample Type I Environmental Concentrate Ground Water (I) .--Surface Water (2) a-z□il(3) _ Other (4) Solid (5) Liquid (6) Sludge (7) Other (8) Comments lc----------.-----____, Organic Chemistry Inorganic Chemistry IParameter _ P§cT:GC/MS V'l\cid: BIN Ext. I 2,4-D , . 2,4,5-TP(Silvex) chlordane I-_ heprachlor hexachlorobenzene Results (mg/I) ------hexachlorobutadiene ------endrin I= lindane _ methoxyc_hlor toxaphene Parameter Results(mg/1) (mg/kg) antimony arsenic barium beryllium cadmium chloride chromium cobalt copper fluoride iron lead 11.JL' PCB s <O,e,o,:,/ffA __ manganese ______ _ -11- FOR LAB USE ONLY .Date Received ~---ff'~tV6 , ff-19-'1 ~ 1.1..t, .Date Extrac~J_;-17-1WP w/t t-19 ,,qr 8 & · Date Analyzed ;:>c<.9;. 7-,;;1.o-'J"?yp I Reported By 1 Date Reported Lab Number I DHS 3191 (Revised 12/93) 982600 - - - - - -- -· - - - - - - mercury nickel nitrate selenium silver sulfates thalli urn vanadium z.inc pH conductivity -------TDS flash point ______ _ EXT/PCB water 159 TCLP Compounds Inorganic Compowuls arseruc -barium -cadmium -chromium -lead - -mercury selenium -silver - - - - Organic Com pounds benzene - - - - - - - - - - - carbon tetrachloride chlordane chJorobenzene chloroform o-cresol m-cresol p-cresol cresol 1,4-dichlorobenzeoe 1,2-dichloroethane 1, 1-dichloroethylene 2, 4-dichloroethylene beptachlor h(:xachlorobenzene hexachlorobutadiene -.. hexachloroethane -_ methyl ethyl ketone nitrobenzene - -pentachlorophenol -pyridine -tetrachloroethylene -trichloroethylene -2,4,5-trichJorophenol -2,4,6-trichlorophenol -vinyl chloride endrin -lindane - -m.ethoxychlor -toxaphene 2,4-D - -2,4,5-TP (Silvex) Results(mg/1) Re,;uits(mg/1) I STATE LABORATORY Of PUBLIC HEALTH P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS BASE/NEUTRAL ANO ACID LAB NO 1qJ1,,75p ~ ll:30~\.-o ◄ C, JI,;),_,; p 1./ wJ>O:Z "-Y.'< I 'I R.2 C\7(,. 'i'/( .,).S J'7 EXTRACT ABLES FIELD# fl'l'\ ··OO;l/., '(!:/).AN •• ~ " A~-<J'"'J', I "71-<H'i .✓• w 1"11.c01tJ-s,.; ,._ i).,o ).0-f,t,.} I COMPOUND TYPE ( I l ( I l ' I l UNITS w, .. n/1' ""/ l ,.--, ' .. n/]~ "n/1,-.. n/ l .. n; l •-"'" N nitrosodimethvlamine IO/ -<~a • -, . II\ . IA .. s (2-ch loroethvl )ether chlornnhenol ohenol '13-dichlorobenzene r / 4-dichlorobenzene ' 2-dichlorobenzene 1ov-JOY ls(Z-ch loroi <nnrnnv] \ether ' I,(,_, xach l oroethane ni troso-di -n....nrl'V"lvlami ne nitrobenzene lithorone trnnhenol 2.4-dimethvlohenol I r (2-ch loroethoxv)methane 4-d i ch l ONV>heno l .2.4-trichlorobenzene naohthalene fachlorobutadiene hloro--01-cresol hexachlorocvclN'\l)ntadiene 114.6-trich lornnheno l chloronaohthalene acenaohthvlene 1 •methvl ohthalate 6-dinitrotoluene cenaohthene 2 4-dinitroohenol sa1 'loSO (t4-dinitrotoluene 1101 '.1'.~0 nitrnnhenol .,01 ,,.c:o fluorene /0/~30 -r R-ch l ornnhenvl ohenv l ether ' l~ethvl phthalate . , ',1 ~-,01-· 4 6-dinitro-o-cresol so, );.c-o I.I\---IA..-f iphenvlamine /0/330 'i1obenzene Cbr~henvlohenvlether hexachlorobenzene ~ lntach l ornnheno l so/11,,:ro enanthrene /;1/ i.'to anthracene ibutvl ohthalate / . / / , luoranthene \ ., \ ' ' ' \ I m"DL - -Estimated value. f{,_o/SOIL- -Actual value is known to be less than value given. -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. The nunoer I -Not analyzed. -Tentative identification., _ -On NROC List of Priority Pollutants. is the Minirr<.111 Detection Limit. m'])L ---- I I I I I I I I n D I I I I I I I I I BASE/NEUTRAL ANO AC!O EXTRACT ABLES C011POJNO nvrene benzidine butvl benzvl ohthalate benz(a)anthracene chrvsene 3 3-dichlorobenzidine bis(2-<ethvlhexvllnhthalate di-n-octvl phthalate benzo(b)fluoranthene benzo(k) fl uoranthene benzo(alnvrene i ndeno( I 2 3-<:dl nvrene dibenzo(a h)anthracene benzo(a.h il=rvlene aniline benzoic acid benzvl alcohol 4-<:hloroaniline dibenzofuran 2-<rethy)Mnhthalene 2-<rethvlohenol 4-<rethvlohenol 2-nitroaniline 3-nitroaniline 4-nitroaniline 2.4 5-trichloroohenol J -Estimated value. STAiE LABORATORY OF PUBLIC HEALTH P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC GIEMICAL ANALYSIS LAS NO 1 au ? ,:;-Ji' ,;J.. 1ao2 '>.\"'i '15?.)..5W q .P.1.,~,- FIELD# n 11. N>).-C. w t'.J)-AO{,,-(,j •• ""·O, :2.-"-,..; (! i) .... -v 'J-(;,..., TYPE < I l I I ) I ./ ) ( ' ) UNITS v,.a/] l.......a... u~/1~ .. n/1........., .. n/l~-- 10/~~o . ,( -IA I A ' , . _._,, l,1a,;o 101:;30 I .• I, .solir..,;o l()/330 /0/.s.~o so/J"5o / / / / \ !,, ,, ..-olu.ro I -I -1, -I A ... ,. 10/=a ~- S'o .,,.<o ; / I / \I/ " ' ' m:n1- H2.0I SOIL. to be less than value given. 4p-,,'9'/_ {l.i)--01tJ-Sw ( .:i. ) V un/ 1' .. " -' IA- I ' K -Actual value is known L -Actual value is known U -Haterial was analyzed NA -Not analyzed. to be greater than value given. for but not detected. The nurrbcr is the Minirrun Detection Limit. 1/ -Tentative identification. ~I -On NROC List of Priority Pollutants. '7VJ<.n7 "',\-tJk)V)(i) I I) .. n; I' .. ' / ' U- 7 ' I STATE LABORATORY Of PUBLIC HEALTH P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS BASE/NEUTRAL ANO ACID LAB NO ~.vv "1 ..17 :1 'I" gq l'-f o, ,-4'/1 '4 v..1.,q1 q V.:J ,</.2 q.ez~-9~ EXTRACTABLES FIELD# 1,",1-4.;iy .,;tJ "11-o~,--<"<· f1ihn1/. A·,. Cl)-c,;; ,., -~.;J-M-Lw /!l),A2o,.,,...,:\ I COHPOUNO TYPE (~) 1A 1 ( .;2..) < I l ( / ) I I ) 11n/ l ' -·· un/ l hm!loo HO/]-,,. . ""/ l , . ......_ /i,n/1 l...,,.i,., V.,n/J).-.,...n UNITS N-nitrosodimethvlamine IQ/;/-IO I ,. 1;4...-1/4...... vL •-'-~ ls(2-chloroethvllether chloroohenol ohenol l3-dichlorobenzene 4-dichlorobenzene 10/< 2-dichlorobenzene IOIA bis(2-chloroisnnrnnv])ether lxachloroethane nitroso-di-n-nrnnvlamine nltrobenzene ~horone trnnhenol 2 4-dimethvlohenol ·s(Z-chloroethoxv\methane 4-di ch lorooheno l , 2 4-trichlorobenzene naohthalene ~achlorobutadiene h loro-<n--ereso l hexachlorocvclnnPntadiene 14 6 trichlor00henol chloronaohthalene acenaohthvlene methvl ohthalate 6-dinitrotoluene "'enaohthene , 2 4-dinitrnnhenol SOI 1050 14-dinitrotoluene 10, '. 1'-10 -nitrnnhenol '>O/tt-<:o fl uorene /0/330 lch lornnhenvl ohenvl ether I ethvl ohthalate J, 4.6-dinitro--o-cresol 50111,,,0 1 i ohenvl amine /0/330 1obenzene Cbrrmonhenvlohenvlether hexachlorobenzene ~ 'ntach l ornnheno l S0l/6':f0 enanthrene ,.,,/:no anthracene ibutvl ohthalate / I I I / / uoranthene ~ \. '\ \. , \ " ... m"])L ' -Estimated value. H,.o/SO/L- -Actual value is known to be less than value given. -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. The nurrber f -Not analyzed. -Tentative identification. _ -On NROC List of Priority Pollutants. is the Mini1TU11 Detection Limit. m])L -- -- I I I I I I I ti I I I I I I I I I I BASE/NEUTRAL ANO ACID EXTRACT ABLES COMPOUND nvrene benzidine butvl benzvl ohthalate benz(a)anthracene chrvsene 3 3---<lichlorobenzidine bis(2---ethylhexvllnhthalate di-n--octvl ohthalate benzo(b)fluoranthene benzo(k)fluoranthene benzo(a)nvrene indeno( 1.2 3--cd)nvrene dibenzo(a h)anthracene benzo(a.h il=rvlene aniline benzoic acid benzvl alcohol 4--ch 1 oroan i l i ne dibenzofuran 2-methvln>nhthalene 2-methvlohenol 4-<nethvlohenol 2 nitroaniline 3-nitroaniline 4-nltroani line 2.4.5-trichloroohenol J -Estimated value. STATE LABOAATORY Of PUBLIC HEALTH P.O. BOX 28047 -306 N. IIILHINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS LAS NO 'IY.:l:5JIY ao~,J? 'lJJ-5l<J I,: n • .:;1,2,5'-j',;,J {!j) ·'t):Jb :Su.) cl) -D2"_,.u, TYPE ( -~ l / ~, ( :2..) ( / l UNITS '""') ~n r.,,,; l 'l.n.<l,n ...,un/1...., .. n I 1 '---"'- /0/~'?0 ' -I , . I, -I - ._,, /11.-:0 /0/.330 I . '/£. lfO S"O/ 101330 /O/.s3o so/t"2'io / / / ,/ ' ,, .... ' l<oh,.,~o I L (.A_ -I -LA- ... ✓ 10/~ ,, S'ol,l.<o I I / / ~, \ \. ' ' fn])J,.. H2.0I Soll.. to be less than value given. "y ,;/54 ,., ,, 71 -,,:JD ,J;t,) ( I l ua/ 1-,_,.,n -, ,/ '\ I , / \ , K -Actual value is known L -Actual value is known U -Material was analyzed NA -Not analyzed. to be greater than value glven. for but not detected. The nurber is the Minirrun Detection Limit. l/ -Tentative identification. ~/ -On NROC List of Priority Pollutants. c..rv -,,~ ;;,t ;•_ --1.J!J'.·, r / 1 ,,nf '"' .. IA- / \ vL 7 \. / I STATE LABORATORY Of PUBLIC HEALTH PO BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS BASE/NEUTRAL AND ACID LAB NO [t?v'J.">'-l<J _Jl'J 1,1;;.~, C}fl.iWl-<rY'l rcJ7 Ov::t.-r -,ir .,.,.,.eJc \ '?'1 I EXTRACTABLES FIELD# r,i)_,,3 /.-r,.,, 'JJ-,-,:/:i-LJt,) vtn"'~,-.uo,.. -~-·l/1~1,J W·"'-Sw ,,,., _ :lo(J-P /J COl1POUND TYPE I J -\ r / l ( ,;:i) ' I l ,.;:i ) ( ii) UNITS .. n/]1.~ un/ l' -.. , ,10/ l lnT.,.._r un/1 ~ ;.,n/1)_,.. .. n/l~n N-nitrosodirrethvlamine IOI 7"0 • • -,,L__, • ,I. -, -i/4..- s(2-chloroethvllether chlornnhenol phenol l3-dichlorobenzene 4-dichlorobenzene .2-dichlorobenzene 1'(2-chloroi •nnrnnvl lether xachloroethane nitroso-di-n.....nrnnvlamine nitrobenzene ~horone trnnhenol 2.4-dirrethvl□henol , is(2-chloroethoxvlrrethane 1_14-dichlo~henol , .2.4-trichlorobenzene anhthalene I 1xachlorobutadiene ch l oro-m-creso 1 hexachlorocvcll'V'Yjntadiene 4.6-trichlornnhenol chloronanhthalene acenaohthvlene rrethvl □hthalate 6-dinitrotoluene acenaohthene 4-dinitrnnhenol S01 'loSO I J4-dinitrotoluene /()I .i~o n1trnnhenol ~OI ;,.co fl uorene /0/"30 lchlornnhenvl □henvlether ethvl phthalate .I, 4 6-dinitro---o-cresol ~1-<:"0 501 1 iohenvlamine /0 ✓330 17obenzene '-braroohenvlnhenvlether ixachlorobenzene ~ ntachlornnhenol .,.-o 111.so enanthrene ,,,, /:r:10 anthracene lbutvl Phthalate 7 I I / / I uoranthene \' \. ' ' ' ... ' rn1>L ' -Estimated value. 1-{,.o/SOI/..... -Actual value is known to be less than value given. -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. The nurrber I -Not analyzed. -Tentative identification. _ -On NROC List of Priority Pollutants. is the Mininun Detection Limit. m"])L ---- I I I I I I I I I I I I I I I I I I I BASE/NEUTRAL ANO AClO EXTRACT ABLES CONPOONO nvrene benzidine butvl benzvl ohthalate benz(a)anthracene chrvsene 3 3--oichlorobenzidine bis (2--<ethvl hexy l) phtha 1 ate di-n--octvl ohthalate benzo(blfluoranthene benzo(k)fluoranthene benzo(a)nvrene indeno(l ,2 3--cdlnvrene dibenzo(a h)anthracene benzo(Q,h, iln,,rylene aniline benzolC acid benzvl alcohol 4--ch l oroan i l i ne dibenzofuran 2--rrethvlnaohthalene 2--rrethyl oheno 1 4--rrethvlohenol 2-nitroaniline 3 nitroaniline 4-nitroaniline 2,4 5-trichlorochenol J -Estimated value. STATE LABORATORY OF PUBLlC HEALlH P.O. BOX 28047 -306 N. WILHINGTON, ST., RALElGH, N.C. 27611 ORGANIC QjEHICAL ANALYS[S LAB NO qy,;J,aU q 'i?,J ,:; 'I, \ iQ p.::i,f"/~ 'IX' r</7 FIELD # l'n _,, 31 • G, (..,,., t'b· ,.V ./1, t'T>•ocl,.-J;,) {'JJ-11J-rnw TYPE ( ' ) l I l (..ll ( l .. UNITS .. o/ I , · " "n I 1 \.,,,,._ ~ .. 0;1 )...-. . HO/\ Jo/i30 IJ -I . "lA___. IL... i ...-,, /,,..,o /0/330 . ' 'Jt..,;o SO/ lo/330 I/O/.J3o so/th'io / / , / ,/ I ' ' • I < 0 /J 1,, .:-o I. -I I 1, . "-., 1al.=o \J, s-o I, 1,,,,:;o / I I / \/ \ \ ' mn1.. HzOI Soll.. to be less than value given. 14'V?_C'IV CiJ ·tXr<,·, I ( ' \ .. n/ 1 .. - / ' LA- / \. I K -Actual value is known L -Actual value is known U -Material was analyzed NA -Not analyzed. to be greater than value given. for but not detected. The nurber is the Hinirrun Detection Limit. 1/ -Tentative identification. ~/ -On NROC List of Priority Pollutants. uv-.... , ,~ (']}.· 'C" (' h .. n/ l '---"-· II ~ . . ,, / . I STATE LABORATORY Of PUBLIC HEALTH (j) P.O. BOX 28047 -306 N. ~ILHINGTON, ST., RALEIGH, N.C. 27611 ---·-. ORGANIC CHEHICAL ANALYSIS BASE/NEUTRAL AND ACID LAB NO ._,,, -o EXTRACT ABLES FIELD# Yn\_u ,o-"111 I TYPE ( L l ( ) ( ) ( l ( l ( ) COIIPOUND UNITS V" □/ j ~aLlrn un/] un/ka .. n/1 .. a/ka ""/ 1 ••□/ka ""/ 1 .. n/ka ,on/ 1 ,o □/ka N nitrosodimethvlamine IO/ i,(30 I ,l - s(2-chloroethvllether chlornnhenol phenol I r-di ch lorobenzene 4-dichlorobenzene 2-dichlorobenzene Ir (2-ch loroi snnrnnvj lether xachloroethane ni troso-di n ....nrnn.vl amine nitrobenzene lliiihorone tr...,henol 2 4-dimethvlohenol I is(2-chloroethoxvlmethane 4-dichlo~henol ,.2.4-trichlorobenzene aohthalene j exachlorobutadiene ch 1 oro-;n-creso 1 hexachlorocvclooentadiene t4.6-trichlornnhenol chloronaohthalene acenaohthvlene (j-imethvl ohthalate 6-dinitrotoluene dcen.:inhthene 2 4-dinitroohenol SOI '~50 m 4-di ni troto 1 uene IOI 330 nitrnnhenol •0I ,,_-:o fl uorene /0/330 D chlornnhenvlohenvlether iethvl ohthalate "' 4 6-dinitro-o-cresol 501 '~--o 1 iohenvlamine /0/330 zobenzene -brNMnhenvlohenvlether hexachlorobenzene 'I llentachloroohenol so/H,S-o Dhenanthrene J/1 /·:n0 anthracene nibutvl ohthalate / luoranthene ' , ' m1)L ~ -Estimated value, 1-{,,.o/sou ... -Actual value is known to be less than value given. -Actual value is known to be greater than value given. U -Haterial was analyzed for but not detected, The nlJTOer ~ -Not analyzed, -Tentative identification. _ -On NRDC List of Priority Pollutants. is the Hinirrum Detection Limit, m'J)L ---- I I I I I I I I I I I I I I I I I I I I BASE/NEUTRAL ANO AC[O EXTRACT ABLES aJIIPOONO ovrene benzidine butvl benzvl ohthalate benz(a)anthracene chrvsene 3,3-dichlorobenzidine bis(2-<>thvlhexvllohthalate di n--octvl phthalate benzo(blfluoranthene benzo(k)fluoranthene benzo(a}nvrene indeno(l 2 3--cdlnvrene dibenzo(a.h)anthracene benzo(o h i l~rvlene aniline benzoic acid benzvl alcohol 4--ch 1 oroan i 1 i ne dibenzofuran 2-mathvlnaphthalene 2-mathvlohenol 4-mathvlphenol 2-nitroaniline 3-nitroa.niline 4-nitroaniline 2 4 5-trichlo=henol J -Estimated value. STATE LABOAATORY OF PUBLIC HEALTH P.O. BOX 28047 -306 N. ~ILMINGTON, ST., ?ALE[GH, N.C. 27611 ORGANIC QlEMlCAL ANALYSIS LAB NO rJV• 1~"'0 FIELD # ""-' IY'l-7i/. TYPE I 'I-) ( ) ( ) ( ) UNITS ' un/ T \.-.u.., .. n/ I uo/kq ""/ l .. n/ko .. n/ I ua/ka Jo/~:?o I - .'\'n /Jt.«:o JOI. '30 . . . , ,1.r:o ,S()/ lo/330 10/.J.:Jo soht.<o / ' / <o!J,_ro 0--- ~ , l"l=o ,,, S'oh 1,,,;o I I ,, ' m1J1- H:z.OI Solt.. to be less than value given. ( ) un/ l .. n/ka K -Actual value is known L -Actual value is known U -Material was analyzed NA -Not analyzed. to be greater than value given. for but not detected. The nuri>er is the Minirrun Detection Limit. l/ -Tentative identification. g; -On NROC List of Priority Pollutants. (i) ( \ HO/ l .. n/kn I ,NC Dcp'utmcnl of. Environmcnl, Huh.h, & N1rur1I Resources SA.tvll'LE A.t~ALYSIS REQUEST St.ate Laboratory of Public He.allh P.O. Box 13047, 306 N. Wilmington St. Solid Wut.c Managcmcnl Divi,ion Raleii;h, North Carolina. 27611-8047 li~Number /I/to 00 I loO(f ol s-O af=00fSi~ Cn'5fl'x Drum s>ie< S~ldICD-001-SL 08/10/98 1020 GRAB 12345678 CD081098, NC D. WILSON ~iteLoc:ition &x ,&,-rl /l/ C--DateCollt _,.,_...___.,._~~~--f+-1~-~--- Collected50ll ORG-CLP Haz.1Idous W asle / Solid Waste K Superfund Sample Type I EnvironmenL1I Concentrate •-- Ground Water (I) Surface Water (2) Soil (3) Otner (4) Solid (5) Liquid (6) Sludge (7) Other (8) 11-----O r g an i c Chemistry Comments Inorganic Chemistry VOA 1 ?:1r.u1Jet'"er . i/P&T:GC/MS Results (mg/I) Parameter Results(rng/l)(mg/kg) l __ ;\,~'.J~B/N Ext. I 2,4,5-TP(Siivox) 1 ~= ~~~~:~~l~r g hexachlorobenzene _____ _ I _ hexachlorobutadiene _____ _ endrin n~= lin<lane mdhoxychlor ~. toxaphene •, ·.', 1- E=-------l FOR LAB USE ONLY I Date Received ;{--/f/-9?14W6 II Date Extracted _________ ~ Dace A..'1alywc! I Repor~~~q.':l.:._!..:::.~::::_,~-.J Date Reno ed · I Lab Nu~ber ~-+9~8_2_G_2_1 __ antimony arsenic barium beryllium cadmium chloride chromium cobalt copper fluoride iron lead manganese mercury nickel nitrate selenium silver sulfates thallium vanadium zinc pH conductivity -------TDS flash point Soil 1 Inorganic. C3'Ef."'f'l:!5 iSSJ Resulls(mg/1) arseruc b~~Pk"FUND JL':.CTiOI~. ca'rlhihlttl 1 ,· .•. , chromium le:td mercury sele:iium silver Organic Compounds benzene c1rbon tetrachloride chlordane chlorobenze:i~ chloroform o-cresoi rn-cre.sol p-cre.30} cresol 1,4-dichlorobenzen::; 1,2-dichloroethane Results(mglJ) ------ 1, 1-dichlorocthyler.e ______ _ 2,4-dichloroethyle~e ______ _ hepta:hlor bexachlo ro ben..ze:1e bex:i.chlorobutadiene ______ _ ..._ bexachloroethane methyl ethyl ketone nitrobenzene pentachlorophenol pyridine tetrachloroethylene trichloroethylene 2,4,5-trichlorophenol ____ _ 2,4,6-trichlorophe:iol ______ _ vinyl chloride endrin lindane methoxychlor toxaphene 2,4-D 2,4,5-TP (Silvex) I NC Dc-/,artmcnt o-:" Environment, Hullh, & Nawral RCliourccs · SMIPLE Ai'IALYSIS REQUEST St.ate Labomory of Public Health P.O. Box 18047, 306 N. Wilmington St. Solid Wute Management Divi,ion Raleii:h_, North Carolina 27611·80,n liteNumber fl:v Oo / (p 'O lo « z:;:n Sample!DNuco-001-SL 08/10/98 1020 GRAB · J. :J. )2345678 CD081098, NC 0. WILSON ( ameofSite C,(s / t'.Y }) ru i::K.' ,$1 b ,Collected By ~SOIL j} ./ ~, :ORG-CLP EXT/PCB Soil iteloc:ition~CJ~"l~Y-·~fv,~J~r,__,<::;..,/'-+-~/IJ~·~G~· ___ DateCollectec ~2 _ __;_ ____ _:_ ___ 2=--:-=====--, ~fund Hazardous W a.ste Solid Waste Sample Type I Environmental Concentrate Ground Water (1) L Surface Water (2) iSoil(3) _· Other (4) - - - - Solid (5) Liquid (6) Sludge (7) Other (8) TCLP Compounds Inorganic Compounds Resulls(mg/1) Comm·ents arse::uc -barium -cadmium -chromium -lead - -mercury selenium -silver - t------,--------1 _- Organic Chemistry Inorganic Chemistry IParameter P&T:GCIMS -i,/4id:B/N Ext. Rc,;ults (mg/I) 11---;:::~TP(Silvex) ---------- chlordane hexachlorobenzene ------11 . heptachJor hcxachlorobuLadiene ~-----cridrin I = lindane _ methoxychlor tox:iphene 1•-lL PCB-; -1- FOR LAB USE ONLY D Date Received ?"-/L/1f$tAJ6 pee,; ?-,;u;-'-'f'T -p 11 Date Extracted &18 ctey,fV' -{;k,l!t II P<:.B ~ 'if-,;i.f-7Y1/ P . . Date Analyzedf,AJ/lj,--),0-f.f'BD m Reported By Date Reported I __ 9_8_2_6_2_2_ Lib Number I DHS 3191 (Rcvi~cd J:/93) Parameter Results(mg/l)(mg/kg) -antimony arseruc -barium -----··--· ---·-··------·· -beryllium cadmium -chloride -chromium -cobalt - -copper fluoride -iron - lead - -m:i.nganese -mer~ury nickel -nitrate -seli!n.ium - silver -sulfates -thallium -vanadium -zinc - -pH -conductivity TDS - -flash point - - Organic Compounds benzene carbon tetrachloride - chlordane Resull5(mg/l) -·---·····-----·--·--·---- chlorobenzene -chloroform - o-cresol -m-cresol - -p-cr.esol cresol - -1,4-dichJorobenzeoe 1,2-dkhloroethane - -1, 1-dichloroethylene -2, 4-dichloroethykne -heptachlor hexaChlorobenzene -· hexachlorobutadiene -..._ hexachloroetbane -_ methyl ethyl ketone nitroben.zene - -pen t.achlo ropbenol -pyridine -tetrachloroeth y I eae -trichloroethylene -2, 4,5-trichlorophenol -2, 4 ,6-trichlorophenol -vUlyl chloride endrin -lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Si]vex) I NC DC'p1.rtmcnt of Environment, Hc.dth, &. Narural Resources SArv!PLE A.t'IALYSIS REQUEST SlAte Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Solid Wute M1.rugcmcm Divi,ion Ralciyh, North C.1rolin1. 27611-8047 litcNumbcr IJto 001 (oO(p ~ s-D SampleIDNum, clo2-3040526-7S8L 08/10/98 1110 GRAB CD081098, NC D. WILSON tame of Site cri-.sfl' X [) fl,{ m ,,;-, le< Collecte<l By -~~~=CLP VOA Soil ~iteLocation _ _,.{)...._,,.,x_,,_fo=r~t~/ __ 7+-' ~N_·~e---~ __ DateCollecte<l ____ -----;:=======---===4====::...., Ha=dous Waste Solid Waste Sample Type I Environmental Concentrate Ground Water(!) L Surface Water('.!) t-Soil (3).~.· Other (4) Solid (5) Liquid (6) Sludge (7) Other (8) Comments TCLP Compounds Inorganic Com pounds Results(mg/l) arse:iic -barium -cadmium -chromium -le:id - -mercury sele!llum -silver - -1-----,-----------1 = --- Organic Chemistry Inorganic Chemistry ·P~~GC/MS f_ Acid:B/N Ext. Results (mg/I) 1---~:::~ TP(Silvex) ------------- chlordane beptachlor hexachlorobenzene ------1 hexachlor~butadiene~----- endrin I lindane methoxychlor toxapht!ne 11 ll=---- D · FOR LAB USE ONLY Date Receive<l ;{--/4 -9710'W6 II Date Ext~acted _________ ~ Date Analyzed --'-Cf_-.c..(3_-_q-"fj---'--7}.2'-=---- 1 Reporte<l By Date Reported _________ _ I Lab Number 982623 I DHS 3i91 (Revi:.ed 11/93) Parameter Results(mg/l)(mg/kg) - - anlimony arsenic barium beryllium cadmium chloride chromium cobalt copper. fluoride iron lead manganese ______ _ mercury nickel nitrate selenium silver sulfates thallium vanadium z.inc pH conductivicy ______ _ TDS flash point Organic Compounds Results(mg/1) ben.zene -- c:i.rbon tetrachloride -chlordane -- chlorobenzene -chloroform -o•cresol -rn•creso! - -p·cresol cresol - -1,4-dichloroben.zene 1,2-<lichloroethane - -I, l-dichloroethylene -2, 4-dichloroethylene -he?tachlor hexachlorobenzene - bexachlorobutadiene -... hexachloroethane -_ methyl ethyl ketone nitrobenzene - -pent.achloropbenol -pyridine -tetrachloroethylene -trichloroethy Jene -2 ,4,5-trichlorophenol -2,4, 6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Silvcx) I NC D9l1rtmcnt oi Environment, Hulth, & Narural Ruourccs SM1PLE Ai'IALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Solid Wutl: Man.agcmcnl Divi,ion Rah!i1,:h, North Carolina 27611~8047 liteNumber Pltv Oo I I / ,-. C0-002-Sl 08/10/98 1110 GRAB (JJ D O ::? r:;-c ' Samp!e!DNu, 12345678 CD081098, NC D. WILSON l'JameofSite "siteLoc.1tion l 1 ,(sfl'v 6 -;fr;,,~ 7) <:.i. · SOIL 1_0✓ l:Y/ 1.!; I[, ,Collected By· ORG·CLP · EXT /PCB Soil /IJ L---DateCol!ectM 5 l lUJc:; .gency: --Hazardous Waste --Solid Waste ~fund TCLP Compounds I Sample Type Inorganic Compounds · Results(mg/1) EnvironrnenL'll Concentrate Comments -arsenic barium - _ Ground Water (I) Solid (5) -cadmium -I_ Surface Water (2) -chromium Liquid (6) -lead .-?Soil (3).· - -mercury Sludge (7) selenium -- -silver -Other (4) ' -Other (8) - - - i Organic Chemistry Inorganic Chemistry - ~ 'Parameter Results (mg/1) Parameter Results(rng/l)(mg/kg) Organic Compounds Rcsults(mg/1) P T:GC/MS antimony benzene ~id:13/N Ext. --arsenic carbon tetrachloride --I 2,4-D ---·-·· barium ·-·-·-·-·-·-· -. --chlordane -----··-·---· --------·-·-··· _ 2,4,5-TP(S,lvex) beryllium -chlorobenzene - 1-chlordane cadmium chloroform -- ' he?tachlcr -chloride -o-cresol hexachlorobenzene -chromium -m-cresol bexachlorObutadiene cobalt p-cresol --endrin ;_, copper cresol ---lind.1no -fluoride 1,4-dichlorobenzene -methoxychlor iron 1,2-dichloroethane --1_ toxaphene lead I, J-dichloroethylene ', --,~ £CS. :i < o, Io ,Pf2t11 -manganese -2, 4'dichloroetbylene mercury beptachlor --nickel hex.achlorobenzene --m--nitrate -hexachlorobutadiene selenium ~ hexachloroethane --silver methyl ethyl ketone --FOR LAil USE ONLY sulfates nitrobenz.ene ~ Date Received "[?-/~-:-~[!JG --thallium pentachloropbenol --vanadium pyridine --tFe-8 !; 'I -?;ti -'f?' p zinc tetrachloroethylene I Dale Extracterle)ja-« \lil'\. !?,..A . -- -pH -tricWoroethylene . Pc.Ks ~-~-W'VP --conductiviry -2 ,4,5-tricblorophenol Date An.Jyzerl,fWA 9-).t)-'($'8£:J -TDS 2,4,6-trichJorophcnol -I Reported By -flash point -vinyl chloride --endrin lindane --Date Re?orterl --methoxychlor I Lab Number 98ZG24 --toxaphene 2,4-D -- --2,4,5-TP (Silvex) I OHS 31?1 (Rc:.vi.\.cd l:::!/93) I NC Depanmcnt c .. f Environment, Hc.allh, & N.1.rural Resources Solid WuLC Managcmcm Divi,ion SMIPLE A.t'l"ALYSIS REQUEST SlAtc Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Ra!ei1:h, North C1.rolina 27611-8047 liteNumber Alto 00 I lo0& ol s-O SampldD Nurr, Collecte<l By_ Date Collected C0-003-SL 08/10/98 1310 GRAB 12345678 · C0081098, NC D, WILSON SOIL .rameofSite ~iteLoC-'.ltion { 1 ,,-s fl' x JJ r K 111 ,'S>le ,, ORG-CLP {)_ 'X forl'.I NC--• l ( lgency: --Haurdous Waste --Solid Waste Duperfund I Sample Type Environmental Concentrate Comments -Ground Water (1) -Solid (5) I_ Surface Water (2) -Liquid (6) 1-Soil (3) i• ... -Sludge (7) ' -Other (4) ,, -Other (8) I Organic Chemistry Inorgan.:c Chemistry t~r Results (mg/I) Parameter Results(mg/l)(mg/kg) _ P&T:GC/MS -antimony Acid: BIN Ext. arseruc --I= 2,4-D . barium . 2,4,5-TP(Silvex) -· --------·-·-·-·-·-·-·-·· .. , .. ,. -···--···----- -beryllium _ chlordane, ·-cadmium I= heptachlor -chloride hexachloro9enzene -chromium hexachlorq_butad iene cobalt --endrin copper 1: -lindane ...... fluoride --methoxychlor iron -toxaphene -lead I -manganese -rnercur; nickel --t--nitrate selenium -silver - FOR LAB USE ONLY -sulfates IDate Receive,! -thallium ?--/¢-9F'(f. vtl 6 -vanadium zinc. -II Date Extracted -pH -conductivity Date Analyzed cz-, e--qe tl.11 -TDS. m Reporte<l By -fla.sh point - - Date Reporte<l -n Lab Number 982625 - - -0 DHS 3191, (Rcviml 1:2/93) VOA Soil 7 -- TCLP Compounds Inorganic Compounds Results(mg/1) arsea.ic -barium -cadmium -chromium -le:id - -:nercury sele:i.ium -silver - - - - - Organic Compounds Results(mg/1) benzene -carbon tetrachloride -chlordane ---·-------chJorobenzene -chJoroform -o-cresol - m-cresol - -p-cresol cresol - -1,4-dichlorobenzene -1,2-dichloroethane -l, 1-dich.Joroethylene -2, 4-dichloroetbylene -heplachlor hexachlorobenzene -hexachlorobutadiene -~ hexachloroethane - -methyl ethyl ketone nitre benzene - -pentachloropbenol -pyridine -tetrachloroethylene -trichloroethylene -2, 4,5-trichlorophenol -2, 4 ,6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphene -2,4-D -2,4,5-TP (Silvex) D NC Department of Environment, He.t.llh, & N1rur.1.l Resources Solid Wute Man.agcmcnt Divi,ion SMIPLE Al~ALYSIS REQUEST St.ate Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Ra!t:.ii,:h: Nonh C1ro!U11 27611-8047 niteNumber JJ;;v Oo I .r=eofSite C,(sfl'y ~iteLoc:ition · {) ';( /4,~ (p V lo 2 s=n Sample ID N, CD-003~SL 08/10/98 1310 GRAB .-. 12345678 CD081098, NC D. WILSON Dn✓ lrJ ,), ;i ,Collected By SOIL ORG-CLP EXT /PC8 Soil 8 Date Collecte tgency: Hazardous Waste Solid Waste ~fund TCLP Compounds ---- I Sample Type Inorganic Compounds Resull5(mg/l) Environrnent.al Concentrate Comments -arsenic barium -_ Ground Water (I) -Solid (5) cadmium - ·~rface Water (2) -chromium -Liquid (6) -lead -mercury r-Soil:(3) -Sludge (7) -selenium -silver -Other (4) -Other (8) - I - -Organic Chemistry Inorganic Chemistry -I Parameter Results (mg/I) Para.n1eter Results(mg/1) (mg/kg) Organic Compounds ResulL5(mg/l) P&T:GC/MS antimony benzene [ i:/.:(c;d: Il/N Ext. -- -arsenic carbon tetrachloride -I 2,4-D barium chlordane ---·--·-·--.. --·-·-··--·--·--·-•-•"> .,, ----------···-·--·-----------_ 2,4,5-TP(Stlvex) -beryllium -chlorobenze=ie ' '"""'"' -cadmium -chloroform __ heptachlor -chloride o~cresol -hexachlorobenune chromium m-cresol = 'hexachlorobutadiene -- -cobalt p-cresol - 1 endrin copper cresol --I · lmdane fluoride 1,4-dichlorobenzene ---_ me\hcixychlor -iron 1,2-dichloroethane -toxaphene .V.2.S"I 2 o, L 9 /dfM1, -lead l, 1-dichJoroethylene I!~ -£ C f3. -manganese -2, 4-dichloroetbylene -mercury -heptachlor nickel hexachlorobenzene ---11--nitrate hexachlorobutadiene -selenium ~ hexachloroethane --silver methyl ethyl ketone --FOR LAB USE ONLY sulfates nitroben.zene I Date Received -- ?-/{C-f$'/lf'WG -thallium pentachloropbenol -vanadium pyridine 1!>!'-P-6-t8 -"16ii,?i -- -zinc . tetrachloroethylene -I Date Extracted_yc._5;. v-..;u;-nw -pH -trichloroethylene P~11-:i.F-~?Vp -conductivity -2, 4, 5-trichl oropheno l Date Analyzed&J -,?t?::9 y,,g& -TDS 2, 4, 6-trichlorophcnol -I Reported By --flash point -vinyl chloride --endrin lindane --Date Reported --methoxychlor I Lab Number --toxaphene 982626 2,4-D -- --2,4,5-TP (Silvex) I DHS Ji 9 l (Revised 12/93) ,, D NC Department ,,f Environment, Health, & Narural Rc.&ourccs SAi\{PLE Ai'IALYSIS REQUEST Slate Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. .Raleii;h, North Carolina 2761 I-R041 Solid Wute Muugcmcnt Divi,ion DiteNumber /I/to 00 I /oO& a s-D CD-004-SL 08/10/98 1345 GRAB SamplelDNu~ l2345b78 CD08l098, KC D. WILSON .rameofSite l!ireLoCJtion Cn'5fl' X Drum ,-;>le< SOIL Collecte<l By -ORG-CLP ()_ x -/2 .-/'./ N C--' I ( Date Collected ltgency: Hwirdous Waste --Solid Waste __0u per fund -- Sample Type I Environmental Concentrate Comments /Jc/21&-?i~ Ground Water (I) Solid (5) --L Sa,face Water (2) -Liquid (6) Cdl/d:z:t-m/ .,v;.;6 fq," -~tapsze,:t.e_.£___ r-Soil (3);'. Sludge (7) -y Other (4) --Other (8) I Organic Chemistry Inorganic Chemistry . t~r Results (mg/I) Parameter Results(mg/1) (mg/kg) _,_ P&T:GC/MS -antimony Acid: BIN Ext. arsen1c --L ~:1:~~(Silvex) -· --·-·· -·-·-·-·-·-·-·--··-··· - barium ····--·-·-----·-----· --bt:.ryllium chlordane cadmium ---I== heptachlor chloride --- r.exachlorobenzene -chromium hexachlorobutadiene cobalt - 1: endrin copper - lindane..~. -fluoride methoxychlor iron - toxaphene load - I -manganese -mercury nickel --t--nitrate selenium -silver. ---- FOR LAB USE ONLY sulfates IDate Received --- -thallium 'ir-///-ffr"r'. tu<:; -vanadium "' zir:c - .Date Extracted --pH <f-8-9!3 -conductivity Date AnJ.lyzed -tJ.j -TDS I Reported By -flash point - -Date Reporte<l - IL.ab Number 982627 - - -I OHS 319! (Revised 1"2/93) VOA Soil 13 l.llilC TCLP Compounds Inorganic Compounds Results(mg/1) arseruc -barium -cadmium -chromium -lead - -mercury selenium -silver - - - - - ~C'ompounds Results(mg/1) nzene ~ban tetrachloride chlordane ---------,- --b-ch!orobenzene -f:-.-""hl o ro form o-cresol - m-cresol --p-cresol cresol - --1../1 ,4-dichlorobenzene ___,_,,-1-; 2-<l i c h1 o roe th an e _.k--i-;T-d i chl oroeth y lene ~4-dichloroethyleoe -heptachlor hexachlorobenzene -hexachlorobutadiene -~ hexachloroelhane ~thy! ethyl ketone nitrobenz.ene --pentachloropbenol _ pyridine ~chloroethylene __kAhcbloroethylene -2, 4,5-trichlorophenol -2 ,4 ,6-trichlorophenol ~nyl chloride endrin -lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Silvex) NC Department of Environment, SMIPLE Al'IALYSIS REQUEST St.ate Labor:alOry of Public Health P.O. Bo,c :!.8047, 306 N. Wilmington St. Ralci1;h_, North Carolina 27611-8047 Hulth, & Na.rural Ruourccs I} Solid Wut.c Marug~mcnt Divi,ion 1/;iteNumber filtv Oo I ltameofSite Cr[sfl''{ ~ v r o 2 c;:n samp1e1n Nu ' C0-004-SL 08/10/98 1345 GRAB 11345678 C0081098, NC 0. WILSON SOIL SiteLoc:1tion t) 'I frir~ rDcu tn .5;/c .Collected By~. DateCollectei. ORG-CLP EXT /PCB Soi I 14 lgency: H=dous Waste Solid Waste ~fund TCLP Compounds ---- I Sample Type Inorganic Compow,ds Results(mgil) Environment.a.I Concentrate Comments arsenic - fl!:lro fM_.l411 barium - Ground Water(!) Solid (5) cadmium i'"''"° Wa<o, ('I -- LJ'//dr0-1V'4 ~1 t1 d, ;,,;....____ -chromium Liquid (6) -lead -~.1:yw1.e-1:--mercury Soil (3) . Sludge (7) selenium --silver - Other (4) -Other (8) - I -. - Organic Chemistry Inorganic Chemistry - I (Parameter . Results (mg/I) Parameter Results(mg/1) (mg/kg) Orrnic Compounds Results(mg/!) ~T:GC/MS -anlimony pnzene 1_ 1d: B/N Ext. -arsenic carbon tetrachloride - __ 2,4-D ' barium chlordane ------·-··-·· ··----···----·· ·-···-·-· ----·--·--·-·-·-·-·-· -2,4,5-TP(Silvex) -beryllium -chlorobenzene chlordaoe -cadmium -chloroform I heptachlor -chloride ~o-cresol hexachlorobenzene chromium ..J<:'.'.: m-cresol -hexaChlorobutadiene cobalt J.CP-Cresol -- I endrin copper ___LL"tres o I - lindane fluoride l ,4-dichlorobenzene rnethbx)'chlor -- -iron 1,2-dichloroethane -- l-1c: toxaphene -lead 1, 1-dichloroethylene -e_c. R :, <O,IO,Rl-nt -manganese -2, 4-d ich I oroeth y Jene --mercury -beptachlor nickel hexachlorobenzene 11= --nitrate hexachlorobut.adiene --selenjum ~ hexacWoroetbane -~ methyl ethyl ketone silver -I FOR LAB USE ONLY sulfates nitrobenz.ene -- ?--I'/-// ?'Vf'Ltu c thallium pentachlorophenol --Date Received -vanadium pyridine -~ f> s-,e -"I\':,"'""' zinc tetrachloroethylene I Date Ex1racted fCB.i ?:-.:i.6-W}IP -- -pH -tricWoroethylene 7't!8s ?~~-9NP . -conductivity 2, 4, 5-t richlorophenol - Date Analyzed &JM-'20-f[?AI;I -TDS 2, 4 ,6-trichlorophenol - · • Reported By -flash point -vinyl chloride --endri.n lincbne --I Date Reported --methoxychlor 982628 --toxaphene Lab Number 2,4-D -- I --2,4,5-TP (Silvex) DHS 3191 (Revised l~/93) I NC Oepartmcnt·of Environment, Hu.Ith, & Nawn.I R~ourccs SA..7v1PLE A.t'l'AL YSIS REQUEST State Labon.tory of Public Health P.O. Box 28047, 306 N. Wilmington St. Solid Wute Man.agemcnt Divi,ion Raleigh, North Carolina 27611-8047 liteNumber Nto 0O/ /oO& ois-O SamplelDNuml CD-005-SL 08/10/98 1245 GRAB 1 12345678 CD081098, NC D. WILSON ( ameofSite Cr/-.-,fl'x D,um S>lc, CollectedBv . SOIL , -. ORG-CLP SiteLocation _..,_t)_""--,,_Xy/r,_~lJ~•-r.~/~---,/t-' ~/IJ-~G-~•---Date Collected_ lrgency: Ha.urdous Waste Solid Waste __0uperfund Sample Type II Envir0nmcntnl Concentrate Comments Ground Water (1) -Solid (5) Surface Water (2) -Liquid (6) Soil Pr Other (4) -Sludge (7) -Other (8) t- i ~--------------~-ln_o_r_!!_a_n_1·-c-C_h_e_m_JS_ -t-ry-~--, U Organic Chemistry ~· I ~p✓r~-~GC/MS R1:sul ts (mg/I) Parameter Results(mg/l}(mg/kg) ~ Acid: BIN Ext. 2,4,D _ 2;4,5-TP(Silvex) ~ ._ chlo_rdru1e heptachlor _ hexa~hlorobenzene _____ _ _ hex~~~~lorobutadiene~----- end'ri.n I -lindin'e = methp'xychlor _ toxaphcne I= - 1=---- D FOR LAB USE ONLY Date Received ?'-lt/-'J</(f? µJc, _, D Date Extracted _________ ~ Date Analyzed q-q -q 'i' 7J.J D Reported By Date Reported D Lab Number __ 9_8_2_6_2_9 __ D DHS 319 I (Revised 12/93) - - ---- - - - - - - - - - - - - - - - - - - - - - -· - - - - - - - antimony arsenic b1rium -beryllium c;admiuor chloride chromium cobalt copper fluoride iron lead manganese rnercur; nickel nitrat~ selenium silver sulfates thallium -vanadium zinc pH conductivity TDS flash point VOA , Soi I 16 TCLP Compounds . Inorganic Compounds Results(mg/1) arsenic -barium -cadmium -chromium -l""d - -mercury selenium -silver - - - - Organic Com pounds Results(mg/1) benzene -c1rbon tetrachloride -chlordane ---ch..Jorobenzene -chloroform -o-cresol -m-cresol - -p-cresol cresol - -1,4-dichlorobenzene -1,2-dichlorC?ethane -l, 1-dichloroethylene -2, 4-dichloroethylene -heptachlor bexachlorobenzene -hexachlorobutadiene - ~ hexachloroelhane - -methyl ethyl ketone nitroben.2ene - -pentachloropbenol -pyridine -tetrachloroethylene -trichJoroethylene -2, 4,5-trichlorophenol -2 ,4 ,6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphene -2,4-D -2,4,5-TP (Silvex) i I NC Department· of Environment, Hullh, & NaOJral R~ourcc& SAi\{PLE Ai'IAL YSIS REQUEST Sta.tc L.tbora.lOry of Public Hullh P.O. Box 28047, 306 N. Wilming1on St. Solid Wut.e Management Divi,ion Ral~ii;h., North Carolina 27611~8047 lsiteNumber /!ICv Oo I (p 1) (o 2 -en Sample ID N, CD-OOS-SL --08/10/98 124S GRAB 12345678 CD081098, NC D. WILSON INameofSite Crr-sft"y :Dcu tr7 .,s;~_CollectedBy SOIL ' _j ~ , ORG-CLP EXT /PCB Soll :ii te Loc;ition ~v~~'f~-~'-"~"--/:i,+7...,. 1--~/IJ~'-'(__"'-___ Date Collecte< 17 .Agency: __ Hazardous Waste __ Solid Waste ~fund TCLP Compounds Sample Type I Environment.al _ Ground Water(!) ·~urface \'{ater (2) 1_ Soil (3) O:• _ Other (4) Concentrate -Solid (5) -Liquid (6) -Sludge (7) -Other (8) t Organic Chemistry I !Parameter _ P§cT:GC/MS _~cid:B/N Ext. Results (mg/I) I I_ ;:1:~~(Silvcx) ----·-----·· chlordane ------11 -_ heptachlor hexachloroben.zene hexachlorobutadiene '------ 1= endri.n .. _ , -_ toxaphene I~ PCB 5 - 1-=---·----1 FOR LAB USE ONLY I Date Received 1[--l'-1--Wvf' tAJG 8-1 S-"t e'V"I .? 6 ... a I Date Extractedf'l?B.f g-,,;J.{,-'/?-Vf' l't.8$ 7-~?-9'3"1/P Date Analyzed ./WA s,,.JO-<JPl/fl I Reported By Date Reported _________ _ I Lab Number 982630 I OHS 3191 (Rcvi~cd 1:2/93) Comments Inorganic Chemistry Parameter Results(mg/l)(mg/kg) antimony arsenic barium beryllium cadmium • ··----· -------- - - chloride chromium cobalt copper fluoride iron lead manganese ______ _ mercury nickel nitrate selenium silver sulfates thallium vanadium z.inc pH conductivity -------TDS flash point Inorganic Compounds arseruc -barium -cadmium -chromium -le,d - -mercury selenium -silver - - - - Organic Compounds benzene carbon tetrachloride -chlordane Results(mg/1) Results(mg/1) ··--·------·-----··-·- chlorobenzene -chloroform -o-cresol -m-cresol - -p-cresol cresol - -1,4-dichlorobenzene -1,2-dichloroethane -1, 1-dichloroethylene -2,4-dichloroethy Jene -heptachlor hexachlorobenzene -hexachlorobutadiene -~ hexachloroethane -_ methyl ethyl ketone nitrobenz.ene - -pentachlorophenol -pyridine -tetrachloroethy lene -trichloroethylene -2 ,4,5-trichlorophenol -2, 4,6-trichlorophenoi -vinyl chloride endrin -lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Si!vex) 'l I NC Department' of Environment, Hullh, & Nao.in! Re1>ourccs SMIPLE At'l'AL YSIS REQUEST State Laboratory of Public He.a.Ith P.O. Box 28047, 306 N. Wilmington St. Solid Wut.c Marue-cmcnt Divi,ion liteNumber Alto OD/ /oO& o/ _s-0 Sample!Dt CD-006-SL 08/10/98 1705 GRAB ----12345678 C0081098, NC D. WILSON Raleigh, North Carolina 27611-8047 rameofSite Cn'.sfl'x Drum ,2!1e, Co!lectedE~~~=cLP VOA Soil Site Loc:ition _.,,,Q"'--.x"'--1-/o-"1/'--''-'-t',-"l--,+<...1.N-=--=C---::;_ __ Date Co!lect-____ -;::======---l=-9-----=:::...., Jgency: Ha,..ardous Waste Solid Waste II Sample Type II Environmental Concentrate Comments Ir Ground Water (]) -Solid (5) Surface Water (2) Liquid (6) -- II-Soil (3)' ' -Sludge (7) -Other (4) -Other (8) ~ Organic Chemistry IPar:uyeter _V_P P&&1T:GC/MS Acid: BIN Ext. I= 2,4-D. 2,4,5-TP(Silvex) chlordane Results (mg/I) I-hep"1chlor = hexachlorobenzene hexachl_o~rObutadiene _____ _ II= 1- endrin lindane· •. methoxychlor taxaphene 11= ---------- 1 FOR LAB USE ONLY Date Received "if'-/{,t-?7j/r;{))6 II Date Extracted _________ ~ Date Analyzed ~9'._-_,_C/_-~Cfwf.___,71'--'-~~-- E Reported By I Date Reported Lab Number 982631. I OHS 3191 (Revised }2/93) Inorganic Chemistry Parameter Results(mg/l)(mg/kg) - - - antimony arseruc barium beryllium cadmium chloride chromium cobalt copper fluoride iron lead manganese ______ _ mercury nickel nitrate selenium silver sulfates thallium vanadium zine pH conductivity ______ _ TDS flash point ______ _ TCLP Compounds Inorganic Compounds arsen1c barium cadmium -chromium - lead - -mercury selenium -silver - - - - Organic Compounds benzene -carbon tetrachloride -chlordane ·---chlorobtll.Zene - chloroform -o-cresol -m-cresol - -p-cresol cresol -1,4-dichlorobenzene -1,2-dichloroethane - -I, 1-dichloroethylene -2, 4-dichloroetbyleoe -hep"1chlor hexachloroben.zene -bexachlorobu"1diene -..._ hexachloroetbane -_ methyl ethyl ketone nitrobenzene - -penLachlorophenol -pyridine -telrachloroethylene -trichloroethy lene -2 ,4,5-trichlorophenol -2,4 ,6-trichlorophenol -vinyl chloride endrin - lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Silvcx) Results(mg/1) Results(mg/1) I NC Oc:partmcnt' of Environment, Hulth, & Nawral Resources SAt\1PLE Ai'IALYSIS REQUEST Slate Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Solid Wute Man.ai,:cmcnt DiviliiOn Ral~illh: Nonh Carolina 27611-8047 ll M'/1 0 I I ( ,, i C0-006-SL 08/10/98 1705 GRAB "itcNumber ~CD D /PQ O !?\C z;--() SampldDNumb/ 12345678 CD081098, NC D. WILSON /1 · _J_ ,._._ <:i. SOIL l'larneofSitc c:,(sfiPY ,vc11 tn '41(, _Collected By_. ORG-CLP EXT/PCB Soil SiteLocation~V~'f~·f,;,-'-')~r,._~,+~-i· -~(I}'-'{..--=-· ___ DatcCollected_ 1 ----;::::=====:.·:..:·=.:.:==2=0====--, O>\gency: __ Hazardous Waste __ Solid Waste ~fund Sample Type D Environmental Concentrate Ground Water (l) D ?Surface W~ter (2) n-Soil (3) ' , Other (4) ;. Solid (5) Liquid (6) Sludge (7) Other (8) Comments 1-.-----,--'--------, Organic Chemistry Inorganic Chemistry TCLP Compounds Inorganic Compounds Results(mg/1) arsenic -barium -cadmium -chromium -lead - -mercury selenium -silver - IParameter Results (mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) _ P_§:T:GC/MS ~cid:B/N Ext. 11 ;:1:~;P(Silvex) --------------- chlordane beptachlor hexachlorobenzene ------hexachlo'robutadiene ~-~--- endrin ~ t'. I = lindane .:,.~' _ methoxychlor __ toxaphene ..k:' PCB s ll=---- I FOR LAB USE ONLY Date Received Y-/L;t-~~ Wo. ~ 6'-L0-'1 l<:M I Date Extractedl~} ?--,:;u;-nyp Pees "il-.:.7-CJrV1> . Date Analyzed 1/JJA ~ .U:"} J{AIJ I Reported By Date Reported I Lib Number --9-8-26_3_2_ I DHS 3i91 (R~vised 12/93) - - ... ., .•.. - - - - -- - - - - - - - - - - - - - -- - - - - - - antimony arseruc barium --·-·-· -·-·-·-·· -· -· -·---, -· _, -- beryllium cadmium. chioride chromium cobalt copper fluoride iron lead mangane~e mercury nickel nitrate selenium silver sul(ates thallium vanadium zinc pH conductiviry TDS ffash point benzene carbon tetrachloride -chlordane ····-·--·-· chlorobenzene -chloroform -o.:.cresol -rn-cresol - -p-Cresol cresol - -1,4-dichlorobenune l ,2-dichloroethanc - -1, 1-dichloroethylene -2, 4-dichloroethylene -heptachlor hexachloroben.zene -hexachlorobut.a,diene - ~ hexachloroetbane - --methyl ethyl ketone nitrobenzene - -pentachlorophenol -pyridine -tetrachlo roe thy !enc -trichloroethylene -2, 4 ,5-trichlorophenol -2, 4, 6-trichl orophenol -vinyl chloride endrin -lindane - -methoxychlor -toxapheoe -2,4-D -2,4,5-TP (Silvex) D NC Depa11mcnL of Environment, Health, & Narural Reiource, SAMPLE Ai~ALYSIS REQUEST State Laboratory of Public Health P.O. Box 18047, 306 N. Wilmington St. Solid Wute Man.agcmcnt Divi,ion Ralci1;h, Nonh C.1rolina 276ll•8047 D,iteNumber It/to 00 I loiJ& a _s-0 SarnpldDNum' CD-007-SL 08/11/98 1900 GRAB -------12345678 CD081098, NC D. WILSON rrameofSite crt-.,,fl'x Drum ,5>·/4, CollectedBy_ ~~~:CLP VOA Soil ..,iteLoc:ition _.._Q......._~X~,,_/!o~,-~r,~/ __ 1,_, ~/lf-~(__..~ __ Dau:Collected ____ -;=======-=--=-=-:.==3=0====::....., tgency: Hazardous Waste Solid Waste Vsuperfund D Sample Type Environmental Concentrate Comments -Ground Water (1) -Solid (5) IL Surface Water (2) -Liquid (6) o-Soil (3) -Sludge (7) j· -Other (4)o -Other (8) n Organic Chemistry IPara~et'er Rcsul ts (mg/I) VP&T:GC/MS [ = Acid: BIN Ext. n~~~= 2,4-D _ 2,4,5-TP(Silvex) heptachlor hexachlorobenzene ------ - chlordane hexachlorobutadiene ~-----Cndrin ,, lindane-·,, methoxychlor toxaphene FOR LAB USE ONLY gDate Received "f5-/</-7't//f7"U/ 6 -g Date Extracted Date Analyzed _q.,__-_,<f'----__,_C/_.f'--'-nJ'-""--- m Reported By Date Reported _________ _ D Lib Number 982G33 u OHS 3191 (Revised 12/93) Inorganic Chemistry Parameter Results(mg/l)(mg/kg) - - - antimony arseruc barium beryllium cadmium. chloride chromium cobalt copper fluoride iron lead manganese mercury nicke! nitrate selenium silver sulfates thallium vanadium zinc pH conductivity ______ _ TDS flash point TCLP Compounds Inorganic Compounds Rcsults(mg/1) arseruc -barium -cadmium -chromium -leod - -mercury selenium -silver - - Organic Compound, Rcsults(mg/1) benzene -carbon tetr:i.chlodde -chlordane ...... , .. chlorobenune -chloroform -o-cresol -m-creSol - -p-cresol cresol - -1,4-dichlorobenzene -1,2-dichloroethane -1, 1-dichloroethylene -2, 4-dichloroethylene -beptachlor hexachloroben.zene -hexachlorobutadiene -... hexachloroethane -_ methyl ethyl ketone nitrobenzene - -pentachlorophenol -pyridine -tetrachloroethy!~ne -trichloroethylene -2, 4 ,5-t richl orophenol -2,4 ,6-trichlorophenol -vinyl chloride endrin - lindane - -rnethoxychlor -toxaphene -2,4-D -2,4,5-TP (Silvex) n NC Ocputmcnc of Envirorunc~t, Hu!lh, & Nawral Rei;;o~rccs Solid Wine Marugcmcnt Divi,ion SAivIPLE Ai'IALYSIS REQUEST SLltc Laboruory of Public Hc.alth P.O. Box 18047, 306 N. Wilmington St. Rali:i1,:h, North C1rolina 27611-8047 E Site Number ~/0_!:~co.D,____,O~Dc.......,/,__~fe~V~( oe-,..2'1---"S:::~·~<'~, Sample ID Numc C0-007-SL 08/11/98 I 900 GRAB , · 12345678 CDO81O98, NC D. WILSON Name of Site Cr(sfl"y rDcu h1 ,5;fc ,Collected By SOIL I / -ORG-CLP EXT/PCB Soil Site Loc:ition _,{)"--"'"x'.-'-fz-'-'-') Gc....,(1--}+· _ _,/IJ'-'-- 1 --'L--:c_ ___ Date Collected 31 I Agency: Hazardous Waste Solid Waste ~fund Sample Type Environmental _ Ground Water (1) E 7u,fac_e Water (2) 1 _ Soil (3)°., Other (4) Concentrate Solid (5) Liquid (6) Sludge (7) Other (8) Organic Chemistry I I Parameter _ P_;!cT:GC/MS _i,,--1;cid:B/N Ext. 2,4-D 2,4,5-TP(Silvcx) hlorda.ne be,ot.achlor Results (mg/I) ~ h 00 exdarinchloroben.zene hexaChlorobutadiene =------ --lindan~: --1 ::~hpohx:,,:hlor I .Jc' PCB $ -C::.0-IOffm_ '-----I FOR LAB USE ONLY E Date Received 5T.-/¢-97//.P,'w6 ~\.t,. 8. 2Q lie)><.,{)-'\ II Date Extracted Peas 1('-::u{;-WVf' II PCBs '3'-~Y-9Y-VP Date Analyzedfir,4 C-u-9fAiJ • Reported By Date Reoorted I . __ 9_8_2_6_3_4_ Lab Number I DHS 3191 (Revi:;cd 12/93) Comments Inorganic Chemistry Parameter Results(mg/l)(mg/kg) antimony arsenic barium beryllium cadmium chloride chromium cobalt copper fluoride iron lead manganese ______ _ mercury nickel nitrate selenium silver sulfates thallium vanadium zinc pH conductivity ______ _ TDS flash point TCLP Compounds Inorganic Com pounds arscruc barium cadmium chromium lead mercury I • se.eruum silver Organic· Compounds benzene carbon tetrachloride chlordane chlorcbenzene chloroform o-cresol rn-cresol p-cresol cresol 1,4-dichlorobenzene 1,2-dichloroethane Results(mg/1) Results(mg/1) I, 1-dichloroethylene ______ _ 2,4-dichloroethylene ______ _ bcptachlor hexachlorobenzene bexachlorobutadiene ... hexachloroethane methyl ethyl ketone nitrobenzene pentachloropbenol pyridine tetrachloroethylene trichloroethylene ------- 2,4,5-trichlorophenol ______ _ 2,4,6-trichlorophcnol ______ _ vinyl chloride endrin lindane methoxychlor toxaphene 2,4-D 2,4,5-TP (Si]vex) D NC Departmer.! of Environment, Hu.Ith, & Natural Re&ourccs Solid Wuie Ma.nagemcm Divi,ion SAMPLE Al~ALYSIS REQUEST St.ate Laboratory of Public Hc.ah.h P.O. Box 28047, 306 N. Wilmington St. Raleiyh, North C.1rollna 27611-8047 E SiteNumber~N~D~' D~=0~0~l_lo~0~6~!l~a_s---z._O __ SampkIDNun CD-008-SL 08/11/98 1900 ·GRAB · . j 12345678 CD08!098, NC D. WILSON NameofSite Cn·.sfl'x Drum .'S>rec Co!lectedBy_ SOIL E Si teLoc:ition _ _,cQ,;,,_..,x,....,.&-"-'-'-,.,c/ce-_-,.., ..,/_ll~L--~·---Date Collected ORG-CLP VOA Soil 33 I E Agency: Hazardous Waste Solid Wast6 _0uperfund TCLP Compounds ·---- Sample Type Inorganic Compounds Results(mg/1) E EnvironmenL1I Concentrate Commenlc; -arseruc -barium Ground Water (I) Solid (5) cadmium ---,_ -chromium Surface \\'.ater (2) Liquid (6) -lead -• -mercury Soil (3) , . , Sludge (7) -selenium ,--'. silver - -Other (4) :, -Other (8) - -I -Organic Chemistry Inorganic Chemistry -- I Parameter Results (mg/I) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) _0&T:GC/MS -antimony --benzene Acid: BIN Ext. arsenic c1rbon tetrachloride --- I 2,4-D "' barium chlordane -·-----· -·-·-.... ··--·-·-·-·-·--·-··· .. ··-· -···---·-·•-·--··· ---·-·-2,4,5-TP(Silvcx) -be!)·llium -chlorobenzene -chlordane c.i.dmiurn chloroform --- -heptachlor -chloride -o-cresol I -hexachJoroben2ene -chromium -· m-ciesol hexachlci"robutadiene cobalt p-cresol -"' --endrin -I copper cresol -,, -- I -lindane J1t -fluoride -1,4-dicblorobe::ize□e . ., -rnethoxy~hlor -iron -1,2-dichloroCthane -toxaphene -lead -I, 1-dichloroethylene --manganese -2, 4-dichloroethylene -mercury -beptachlor nickel hexachlorobenzene --- I --nitrate -hexachlorobutadiece selenium ~ hexachlor6ethane --silver methyl ethyl ketone --FOR LAB USE ONLY sulfates nitrobenzene --I Date Received -thallium penLachlorophenol '?-/4"-yfJ/,?; wG - -vanadium pyr:idi.ne . "' -zinc tetrach..loroethylene --I Date Extracted -pH -trichloroethylene <?-1-qf 1J.1 -conductivity -2, 4,5-trichlorophenol Date Analyzed -TDS 2,4 ,6-trichJorophenol -I Reported By -flash point -vinyl chloride --endrin lindane --Date Reported --methoxychlor I Lab Number 982635 --toxaphene 2,4-D -- --2,4,5-TP (Silvex) I DHS 3191 (Revised 1"2/93) D NC Departmc~t of Environment, Health, & Nawral Re1,ourcc, Solid WuLe Marugcmcnt Divi,ion SA.i\1PLE A.L'IAL YSIS REQUEST St.a.te Laboratory of Public He.11th P.O. Box 28047, 306 N. Wilmington St. Rali!i1;h_, North Cuolina 27611-8047 D Siu: Number __,_/0-'-'r,""~v,__,,_O'-'v"-</<--...:(p_.v'--'('-"o'--<"~'l---'5='----<'--,,'-' Sample ID Nurr C0-008-SL 08/11/98 1900 GRAB · J._ ,...._ <:i. 12345678 C0081098, NC O. WILSON Name of Siu: C,(sfl'Y !{/Cu tn 0!.£, _Collecte<lBy _ SOIL _ 34 0 tf\ fl ~ I!/ /' ORG-CLP EXT /PCB Soll SiteLoc:ition t'./ '{UJCG, fr L----Dau:Collected ~~~~= .... ~-~~-='-----~-----------------0 Agency: __ Hazardous Wasu: __ Solid Wasu: ~fund Sample Type 0 Environmental Ground Water (1) g _ Surface Wa:er (2) a ✓ Soil (3). _ Other (4) · . ,,. Concentrate Solid (5) Liquid (6) Sludge (7) Other (8) I Organic Chemistry Comments Inorganic Chemistry TCLP Compounds Inorganic Compounds Results(mg/1) arsenic -barium -cadmium -chromium -lead - -mercury selenium -silver - - - - I Parameter Results (mg/I) Para.meter Results(mg/l)(rng/kg) Organic Compounds Results(mg/1) _ P§cT:GC/MS _L.---'t\cid:B/N Ext. I ---· 2,4-0 . _ 2,4,5,TP(Silvex) chlordane _ hept.ichlor I _ hexachlorobenz.ene _____ _ hexachlorobutadiene ~------ _ liBdajie; •~ _ methoxychlor _ toxaphene .,.1c PCS s FOR LAB USE ONLY I Date Received :{-/,'/-f?W, {,{,/ G f{cP,-(3 -2.0 A@',::n'\ I Date Extracted~ ?-~6-9?vp ~$' 1!-21 -97'VP Date Analyzed /3IJ/lj,,),I-')~ I Reported By ·Date Reported--~-------1 Lab Number 982636 I D\lS JJ9t (R<Yi>eJ 12193) - - --- - - - - -. - - - - - - - - - - - - - - - - -- - - antimony arseruc barium -·-·--·-·-·--·-·-·--·---· beryllium cadmium chloride chromium cobalt copper fluoride iron lead manganese mercury nickel nitrate selenium silver sulfates thallium vanadium zinc pH conductivity TDS !la.sh point benzene carbon tetr::i.chloride -chlordane -·------··--··----·······-chloroben.zene - chloroform - o-cresol -m-cresol - -p-cresol cresol - -1,4-dichlorobenzene -1,2-<lichlOroethane -I, 1-dichloroethylene -2, 4-dichloroetbylene -heptachlor hexachlorobenzene hexachlorobutadiene -------- w,. hexachloroethane -methyl ethyl ketone nitrobenzene - -pentachlorophenol -pyridine -tetrachloroethylene -trichloroethy lene -2, 4, 5-tri chJ orophenol -2,4, 6-trichlorophenol -vinyl chloride endrin - lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Silvex) -------. I NC Dqartmcr,t of Environment, Heallh, & Nawrai Rci;ourcc& SAlvIPLE Ai'IALYSIS REQUEST SI.Ate Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Solid W.i.,te_ Management Divi,ion Raldi::h, North Carolina 27611-8047 lsite Number !tit O O O I lo L) (p a _s--0 SampldD Numb, CD-009-SL 08/12/98 1450 GRAB · · . J 12345678 CD081098, NC D. WILSON IINameofSite Cr-,'.5fl'x Drum ,21ie, Collecte<lBy_ SOIL II / ORG-CLP Site Loc:ition _ _,,c;,O'-.,<x'--1-&-'''-','---{,.c.,,,___-1-( _,fl;_:_'_,L---c: 4 ::_ __ Dale Collected VOA Soil 36 ( .Agency: --Hazardous Waste --Solid Waste _0uperfund TCLP Compounds Sample Type Inorganic Compounds Results(mg/1) I Environmental Concentrate Comments arsenic -barium - -Ground Water O) -Solid (5) -cadmium I_ -chromium Surface W~ter (2) -Liquid (6) -le:id -mercury Soil (3) < Sludge (7) selenium m-,., •. --silver - -Other (4)·,. -Other (8) - It . - -Organic Chemistry Inorganic Chemistry - I P~r Results (mg/I) Par:.uneter RcSul ts(mg/1) (mg/kg) Organic Com pounrls Results(mg/1) _ P&T:GC/MS -antimony -benzene Acid:B/N Ext. arsenic c1rbon tt::trachloride ---11-: 2.4-D . -, ~ barium chlordane '~ .. ·--··--_, ..... ·-·-··· •··-·--··-.............. _ ----· ---•-·-----------·- 2,4,5-TP(Silvex) · -beryllium -ch..lorobeIW!ne chlordane• cadmium chloroform --- II= heptachlor chloride o-cresol -- hexachlo roben2ene -chromium m-cresol bexaChlctrabutadiene -cobalt p-cresol --- endrin ,i; copper cr;:sol . ;, ' . I -lindane :t:'. -- -fluoride 1,4-dichlorobenzene methoxYChlor -- -ircn l ,2-dichloroet3ane -- -toxaphene -lead I, 1-dichloroethylene - I --manganese -2 ,4-dichloroethylene --mercury hepc1chlor -nickel hexachlorobenzene --- ll-nitrate hexachlorobutadiene --selenium ~ hexachloroethane --silver methyl ethyl ketone --- FOR LAB USE ONLY sulfates n.itroben.zene . II Date Received --thallium pent.achloropbenol ¥-/?/-CZY'13IJ/b --vanadium pyridine --- -zrnc tetrachloraethylene -II Date Extracted -pH - - tricbloroethylene 1J,} -conductivity 2 ,4,5-trichlorophenol 9-C{-Cff - Date Analyzed -TDS 2,4, 6-trichlorophenol -I Reporte<l By -flash point -vinyl chloride -endri.n -lindane -- Date Reporte<l --methoxychlor I Lib Number 982637 --toxaphene 2,4-D -- --2,4,5-TP (Silvex) I OHS 3191 (Revi:;cd 12/93) NC bepartmcilt oi ~nvironrncnt, Hcallh, & Nawral Ruourccs SAJ'vIPLE Ai~AL YSIS REQUEST State Laboratory of Public He.allh P.O. Box 28047, 306 N. Wilmington St. II Solid Wute Man.agcmcm Division Ralc:igh_, Nori.h Carolina 27611-8047 llsiteNumber Jltv Oo I aNameofSite Sitel.oc:itio□ Crysfl'y e xfrir~ fe Q (o 2 'L(; Sample ID Nun CD·009·SL 08/12/98 1450 GRAB ' · 12345678 CD081098, NC D. WILSON 1) <-J. ' SOIL '~CU lr) ,..,), 1£ ,Collecte<lBy-, ORG·CLP EXT/PCB Soil !Ji/' 37 IV L---Dat.eCollected .. . -. - UAgency: Hazardous W ast.e Solid W ast.e ~fund TCLP Compounds ---- 0 Sample Type Inorganic Compounds Results(mg/1) Environmental Concentr.ite Comments -arseruc barium -Grouod Water (I) Solid (5) cadmium u= Surface·Water (2) -- -chromium Liquid (6) -le:i.d m 7soil (3)- - -mercury Sludge (7) selenium -- -silver -Other (4) -Other (8) - I - - Organic Chemistry • Inorganic Chemistry - I Parameter Results (mg/I) Parameter Results(mg/1) (mg/kg) Organic Compowuls Results(mg/1) ~T:GC/MS antimony benzene -- I _ 1d:B/N Ext. arseruc carbon tetrachloridt --2.4-D .. barium chlordane ·--· ·-------·-·-------· ·-----·-·-•-·-· -·-·-·--··-----·· 2,4,5-TP(Silvex) beryllium chlorobenzene ---· chlordane cadmium chloroform -- 11 beptachlor -chloride -o-cresol hexac~oroben.ze:1e -chromium -m-cresol -hexachlorobut.adiene cobalt p-cresol -- I -endrin~ -copper -cresol -li□dane fluoride 1,4-dichlorobe□zene -- -methoxychlor -iron -1,2-dicWoroethane I -toxaphene -lead 1, 1-dichloroethylene - .Jc' e_c. 8. s -<:O, /0 fP>"-· -m10ganese -2,4-dichloroelhy kne mercury beptachlor --- nickel hexacWorobenzene --I - -nitrate hexachlorobutadiene --selenium ' hexachloroethane -- -silver me1hyl ethyl ketone - I FOR LAB USE ONLY -sulfates nitrobenzene - -thallium pentachlorophenol - Date Receive<l 7--"/t,,!-7'.f'~6 vanadium pyridine --~0-Z..0-"<0 -zmc tetrachloroethylene. I Date Extracted ~ 5!-~6.---LJ'i?Vf' - -pH -trichloroethylene ~cBs 8-.;1$'-1.{VP -conductivity. -2 ,4,5-trichlorophenol Date Analyz 8AJft:8'.-~-'lf. -TDS 2, 4,6-trichlorophenol -I Reported By -flash point -vinyl chloride --endrin lindane --I Date Reported --methoxychlor 982638 --toxaphene Lab Number 2,4-D -- --2,4,5-TP (Silvex) Df!S 319! (Revi:.,:d 1'2/93) I I ,. 0 NC Ueputmc-1,t of Eiwironmcnt, Health, & Narural Ruourccs SAMPLE Ai~ALYSIS REQUEST St.ate Laboratory of Public Hullh P.O. Box 23047, 306 N. Wilmington St. Solid Wut.e Ma.rugcmcnt Divi,ion Raleii;h, NoM C.1rolin1. 27611-8047 R Al /I() 00 / IO 1 -::, c-;Q Sam l·IDNu1· CO·Ol2-SL 08/11/98 1720 GRAB itt:Number fl[& f(} If' 0-> c P ~ 1234567 8 CDO81O98 NC O. WILSON lfameofSitt: C,.-'/-,sfl'x Drum :S>-/4:., CollectedBy_ ~~~~CLP VOA ' · Soil SiteLoc.:ition _ ... Q,..._r',X,_,_/4=1/~r~r.=/ __ 7+·,~/_1/~[._..~•---Datt: Collectea ____ --:====-----_:1:_4~2 - Jgency: Haurdous W astt: Solid Wastt: _0uperfund TCLP Compounds Sample Type II Environmental Concentr..1te Comments It Ground Water (1) Surface-Water (2) -Solid (5) -Liquid (6) lt-Soil (3) ·: ·• .. , Other (4),:i, --Sludge (7) -Other (8) 1-----,---------'----j Organic Chemistry Inorganic Chemistry Aciu:B/N Ext. u--2,4~0 ,,. u ____ 2,4,5-TP(Silvex) ~. 'chiordahe heptachlor hexachlorobenzene Results (mg/I) ------hexachlc;>robut.adiene _____ _ t- endrin . lindane 1 methoxychlor toxapht!ne I FOR LAB USE ONL y Date Received y-/£/-91/ltu}t;" IDale Extracted··---------~ Date Analyzed r-q~C/f 1J,,f I Reported By 1 Date Reported Lab Number 982639 I DHS 3191 (Revised 12/93) I Parameter Results(mg/l)(mg/kg) --antimony arsen.ic -badum ., ...... -,, ......... ·······-···-·--·-··· -beryllium cadmium --chloride - c~omiurn -- cobalt - -copper . fluoride - iron -lead - -nunganese --macury nickel - nitrate -selenium -silver -sulfates -thallium -vanadium - 21.IlC - -pH -conductivity TDS - -flash point - - - - Inorganic Compounds arsenic -barium -cadmium -chromium -lead - -mercury selenium -silver - - - - Organic Compounds benzene carbon tetrachloride -chJordane Results(mg/1) Results(mg/1) ---··---·-··-------chlorobenze~t:! - chloroform -o-cresol -m-cresol -- -p-cresol cresol - -1,4-dichlorobenzene -1,2-dichloroethan.! -1, 1-dichloroethylene -2, 4-dichloroethylene -beptachlor hexachlorobenzene -hexachlorobutadiene -..,_ hexachloroetbane -_ methyl ethyl ketone nitrobenz.ene - -pentachlorophenol -pyridine -tetrachloroethylene -trichloroethylene -2, 4 ,5-trichlorophenol -2 ,4,6-trichlorophenol -vinyl chloride endrin - lindane - -methoxychlor -toxaphent! -2,4-D -2,4,5-TP (Silvex) D NC Depanmc,'1C of Environment, Health, & Nawral Resources Solid Wu~ Muugcmcnt Divi,ion SMIPLE Ai'IALYSIS REQUEST St.ate Labontory of Public Health P.O. Box 28047, 306 N. Wilmington St. Raleii;h_, North C.1rolina 27611-8047 Esite Number __,ft!t--'"<C'-'-D'--"0'-'D"--</,__"'(p__,7)'---(._.o:.....,;c(('l--'S--'---'--C'.,_, Sample ID Nu• C0-012-SL 08/11/98 1720 GRAB · ~ r-;,. ~:j_ . 12345678 CD081098, NC D. WILSON NameofSite C,t~sJl'Y r/ ;/QJ M ,.5,;i;;,,CollectenBy_ SOIL m ~ j/ l -/I) /' ORG-CLP EXT /PCB Soil . SiteLoc:ition ~tl~~K~·~tv=G_,_('.i,._1}_,__~-~~L----~ ___ DateCollecte<l ~---------1_4_3 _____ _ mAgency: __ Hazardous Waste __ Solid Waste ~fund Sample Type m Environmental Concentrate _ Ground Water (1) ,_. Surface ,i,;ater (2) 17soil(3) ".: _ Other (4) ; Solid (5) Liquid (6) Sludge (7) Other (8) I l Organic Chemistry I P~rameter P&T:GC/MS V'f\cid:B/N Ext. I :_:_:_: ;:::~-Thsi!vex) chlordarie heptachlor hexachlorobenzene Results (mg/I) ------hexachloI"obutadiene -,·• ~-----1 1-.- endrin .~. I == :::;";~~or = toxapht:;~ I -1e_ PCB$ I FOR LAB USE ONLY I Date Receive,:! ?'-/",t-'r,?J//?'r,JC, . f,:,-Pt e,,2..O ..ct'l \c.-1'1\ I. Date Extracted ft:-B~ .V-.;;:i~-9YVP 'PCBs '?l-.:{Y-93VP Date AnalyzenAIJAf~:J./ -9 P8/J I Reported By Date Reporte,l _________ _ I Lab Number 982640 I DHS 3191 (Rcvi:;e<l 1::193) Comments Inorganic Chemistry Parameter Results(mg/l)(mg/kg) - - - - - antimony arsenic barium beryllium cadmium chloride chromium cobalt copper fluoride iron lead m111ganese ______ _ mercury nickel nitrate selenium silver sulfates thallium ·vanadium zinc -pH conductivity ______ _ TDS fla..sh point TCLP Compounds Inorganic Compounds arsenic -barium -cadmium -chromium -le:id - -i:uercury selenium -silver - Organic Compounds benzene carbon tetrachloride -chlordane Results(mg/1) Resu!L,(mg/1) ---·····-·--··-·····-·-chlorobenzene -chloroform -o-cresol -m-cresol - -p-cresol cresol - -1,4-dichlorobenzene 1,2-dichloroethane - -1, 1-dichloroethylene -2, 4-dichloroethy lene -heptachlor hexachlorobenzene -hexachlorobutadiene - ... hexachloroethane -_ methyl ethyl ketone nitrobenzene - -pt:ntachloropbenol -pyridine -tetrachloroeth y lene -trichloroethylene -2, 4,5-trichlorophenol -2, 4 ,6-trichlorophenol -vinyl chloride endri.n -lindane - -methoxychlor -loxaphene 2,4-D - -2,4,5-TP (Silvcx) 0 NC Department of Environment, Heallh, & Nawn.I R~ourccs Solid Wine Management Divi,ion SAi'vlPLE Ai',TALYSIS REQUEST St.ate Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Ra!cii:h, North Carolina 27611-8047 Rite Number Nto OD I loO& a s-D Sample ID Nu, C0-014-SO 08/12/98 1015 GRAB , 12345678 C0081098, NC 0. WILSON ,rameofSite l\itel..ocation Cn·5fl'x Drum ,2ife, t)_ i In,-(' J N C-- Collected By_ Date Collected ORG·CLP VOA Sediment 48 ' ' --I ' ltgency: --Hazardous Waste 1 --Solid Waste _0uperfund TCLP Compounds Sample Type Inorganic Com pounds Results(mg/1) m Environmental Concentr.1tc Comments -arsenic ·~efro/eum barium - Ground Water (1) Solid (5) -cadmium --IL Le)IWUl:q 'rer:ti V!'----chromium Surface Water (2) Liquid (6) -le,d - ~-0/1 .fl? c,le.) ... -mercury II Soil (3) i: Sludge (7) selen.ium -I - ' -silver Other (4). ' Other (8) ; --- I - -Organic Chemistry Inorganic Chemistry - IP~r Results (mg/1) Parameter Results(mg/l)(mg/kg) · Organic Compounds Results(mg/1) _ P&T:GC/MS -antimony -benzene Acid:B/N Ext. arsenic carbon tetrachloride ---I= 2,4-D ., . -· .. barium --------·· ., ___ , _____ .. ----chlordane · 2,4,5-TP(Silvcx) ·-······· ---····--..... , .... -··--- -beryllium -chlorobenzene chlordru1e : cadmium chlor0form --- I= hept.ichlor -chloride -o-cresol hexachJoroben.zene -chromium -rn-cresol he:.achloro bu t.idiene cobalt p-cresol ---_ endrin .,,.--copper -cresol I= lindane · · fluoride 1,4-dichlorobenzene --_ methoxychJor iron 1,2-dichloroethane -- -toxaphene -kad 1, 1-dichloroethylene - I -manganese -2, 4-dichloroetbylene -mercur; -bept.ichlor nickel hexachlorobenzene ---1--nitrate hex.:ichlorobutadiene -~eknium ~ hexachloroetbane --silver methyl ethyl ketone --FOR LAB USE ONLY sulfates nitrobenzene IDate Received --thallium pentachloropbenol 1?---/'f-ff~G --· -vanadium pyridine -zinc tetrachloroethylene -- .Date Extracted" -pH -trichloroethylene 1-10 ~qr M -conductivity -2, 4, 5-tri chl orophenol Date Analyzed -TDS 2, 4,6-trichlorophenol - .Reported By -flash point -vinyl chloride --endrin. lindane --Date Reported -. -methoxychlor • Lab Number 982641 --toxaphe□ e 2,4-D -- --2,4,5-TP (Silvex) I DHS 3191· (Ri:viscd 12/93) I I NC Department of Environment, Health, & Natural Ruourccs SAi'vIPLE Ai'IALYSIS REQUEST SLB.tc Laboratory of Public Health P.O. Box 28047, 306 N. Wilmingt'on St. Solid Wule Management Divi,ion Raleit::h, Nonh C1rolu1127611-8047 lite Number IICv Oo f ~ D {o ::? i:;-n Sample ID Nu, CD-014-SD 08/12/98 1015 GRAB C · .J_ " . 5'-f. , 12345678 C008!098, NC D. WILSON lfameofSite ~(Sjl'Y/ ,/,!CtJ Ir/ i-.!J.t.£, _Collecw:IBy _ ORG-CLP ~iteLoc:ition ~[J~~x'.~t-VG._(;:;,_7_,__~/l) __ (____~ ___ Date Collectec g..gency: __ Ha=dous Waste __ Solid Wa.ste -~fund Sample Type D Environmental Concentr.ite Ground Water (!) IL Surface Water (2) It:: Soil (3) . ''.' / Other (4} • Solid (5) Liquid (6) Sludge (7) Other (8) Comments EXT/PCB Sediment 49 TCLP Compounds - Inorganic Compow1ds Resul ts(mg/1) arsenic -bariuni -cadmium -chromium -lead - -mercury selenium -silver· - -· Ii--· --:-------r--------1 - II Organic Chemistry Inorganic Chemistry tararncter P&T:GC/MS V'l\cid: BIN Ext. l-2,4-D . , L 2,4,5-TJ:(Stlvex) chlordane . Results (mg/I) I-= heptachlor hexachlorobenzene _____ _ hexachl0'robutadiene r= endrin lindane ,.;,~ ~ methoxychlor _ toxaphene I~ PCB-; t- ------ FOR LAB USE ONLY .Date Received ?---JL/--<j~'f"WC ~r--ei~ q l"..IY\ • Date Extracted l'CQi,-1{-'-9YYP P(!/Jr '?-.:r?-'IY'Vp Date Analyzcd(),Jlf?-ol/ :gj,;ifj' IR;ported By Date Reported _________ _ IL.ab Number 982642 Parameter Results(r.1g/l) (mg/kg) -antimony arsenic -barium ---------- -beryllium ca.dmium -chloride -chromium -cobalt - -copper fluoride -iron -lead - -manganese -rnercur; nickel -nitrate -selenium -silver -sulfates -thallium -vanadium - ZillC - -pH -conductiviry TDS - -flash point - - -- - - - Organic Compow1ds benzene carbon tetrachloride -chlordane --·- chlorobenzene --chloroform -o-cresol -m-cresol - -p-cresol cresol - -I ,4-dichlorobenzene 1,2-dichloroethane - -I, 1-dichloroethylene -2, 4-dichloroetbylene -beptachlor · hexachlorobenzene -bexachlorobutadiene -"" hexachloroetbane -_ methyl ethyl ketone nitrobenzene - -pentachloropbenol -pyridine -tetrachloroethylene -tricWoroethylene -2, 4,5-trichlorophenol -2, 4,6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphe□e 2,4-D - -2,4,5-TP (Silvex) Results(mg/1) ···----···---... ·······-·--- ! ' i NC Department of Environment, Hu.Ith, & Nawral Resources S~lid Wane Management Divi,ion SMIPLE Ai~ALYSIS REQUEST State Laboratory of Public He..alth P.O. Box 28047, 306 N. Wilmington Sl. Ralcii:h, ~orth C.1ro!ina 27611-8047 II It/ fi O j 1 1 :::-i c-Q C0-015-SO 08/12/98 1040 GRAB 1fite Number --'"'-'-'t,,'-'[.,,_)_,0"'--"''--L.·_,f"'-<0=-0...,(f-"'-VI'--'->::_ ' __ Sample ID Nu 12345678 CD081098, NC D. WILSON g'ameofSite 'titeLoCJ.tion Cn·-5 fl' x [) {l,(/n .5~ ie. Collected By. ORG-CLP Q x -/4,-;;/ NC-( ' 7 DateCollecte-_o:-jy tfi- >z,i,~U:A Soil (3) ' Sludge (7) II - Other (4) ~, --Other (8) I Organic Chemistry Inorganic Chemistry r~erer. Results (mg/I) Parameter Results(mg/1) (mg/kg) _ P&T:GC/MS -antimony Acid: BIN Ext. arsenic --· -L 2,4-D, . barium ·-··-------•.. 2,4,5-TP(Silvex) -··-··--·-·-····-·-·----.. -· .. '·---- -beryllium . chlordane· cadmium -• - I heptacltlor -chloride hexachlo ro ben1.ene chromium -hcxachlorobutadiene cobalt -.·:, . -endrin ,._ copper I linci3.ne ~/ - -fluoride methoxy~hlor iron . -toxaphene lead - I --manganese -rnercur; nickel --l--nitrate selenium -silver -FOR LAB USE ONLY sulfates I Date Received - -thallium ?-/~ -2YY4WG -vanadium zinc -I Date Extracted -pH 9-10~9~ -n-::1. -conductivity Date Analyzed -TDS I Reported By -flash point - -Date Reported -I Lab Number 982643 - - - VOA Sediment 51 .j.U.J.;,., TCLP Compounds Inorganic Com pounds Results(mg/1) arseruc -barium -cadmium -chromium -ie:id - -mercury I . se.enium -silver - - -:,• --. - Organic Compounds Rcsults(mg'I) benzene -carbon tetrachloride -chlordane --·-.. --· chlorobenzene -chloroform -o-cresol -m-cresol - -p-cre:sol cresol - -1,4-dichlorobenzene 1,2-dichlorocthane - -1, 1-dicltloroethylene -2, 4-dichloroethylene -heptacltlor hexachlorobenzene -hexachlorobutadiene -' hexachloroetbane - -methyl ethyl ketone nitrobeazene --pent:J.chlorophenol -pyridine -tetrachloroethylene -trichloroeth'y lene -2,4,5-trichlorophenol -2, 4,6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphene -2,4-D -2,4,5-TP (Silvex) I I OHS 3191 (Revised 1'2/93) -· I NC Department of Environment, Health, & Narural Re1>ources Solid Wute Man,.gcmcnt Divi,ion SMIPLE Ai~ALYSISREQUEST Slate Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Raleii;h, North Carolina 27611-8047 liteNumber lli;v Ov I le D lo 2 s-::n Sample ID Numb CD'015-SD 08/12/98 1040 GRAB , 12345678 CD081098, NC D. WILSON rameofSite Site Location Cr[sf,,,v 61/2,~ :Dcu IJ4 ,,s;~ ,Collected By_· . 0RG-CLP EXT /PCB Sediment /IJ L--Date Collected 1 -52 .gency: Hazardous W a.ste Solid Waste ~fund . TCLP Compounds ---- D Sample Type Inorganic Compounds Result.s(mg/1) Environmental Concentrate Comments -arsenic barium /kfro( J ,l,,U,1:-.:_ - Ground Water (I) -Solid (5) -cadmium tr C,{!k_,f t_L/1,v/ /1 ~-,,;,------chromium Surface Water (2) -Liquid (6) -lead . ' / ?:JfA.-5 /? {_,0& e,( -mercury u-Soil (3) ,._/ -Sludge (7) selenium -V silver /other (4/;, - -Other (8) - ~ - - Organic Chemistry Inorganic Chemistry - IParameter Results (mg/I) Parameter Resul t.s(mg/1) (mg/kg) Organic Compowuis Result.s(mg/1) P&T:GC/MS -antimony -benzene -,/4id:B/N Ext. arsenic carbon tetrachloride --I-2,4-D .. barium chlordane -------------~-··-·------···-·-····--... -···-· 2,4,5-TP(Silvcx) -beryllium -!.:hlorobcnzene -. chlordao'e cadmium chlorofonu. --- I heptachlor -chloride -o-cresol hexachlorobenzene chromium m-cre.'.iol hexachlor0butadiene -- -cobalt p-cresol (.,, -- I endrin ' copper cresol . -'\: --hndane J :, • -fluoride 1,4-dichloroben..zene methoxycnlor -iron 1,2-dichloroethane -... --toxaphene -lead 1, 1-dichloroethylene I.Jc --£C..B. :i < Q. LO f¥?t!< -manganese -2, 4-dichlorocthylene r mercury beptachlor -· -nickel hexachlorobenz.ene --- 11-· nitrate hexachlorobutadiene -selenillrn - ' hexachloroethane -- -silver methyl ethyl ketone -FOR LAB USE ONLY sulfates nitrobenzene I Date Received '?-/ lj -czzvgwc -- -thallium pentachlorophenol -vanadium pyridine --~ e,-io>ie>"'-'Yl -zrnc lf:lrachloroeth y 1 ene I Dale Extracted {!_C.Bs <Jl-::i.6-'l?YP - -pH -trichJoroethylt:ne 'i't'8f ?-31-9i"ll[ --coriductivity -2, 4,5-trichlorophenol Date Analyzed f/µA K-'.J.V--9,!"A TDS 2, 4,6-trichlorophcriol --I Reported By -flash point -vinyl chloride --endri.., lindane -- 1 Date Reported --methoxychlor 982644 --toxaphene Lab Number 2,4-D -- --2,4,5-TP (Silvex) OHS 3191 (R~vis!!d_l2/93) I NC Dcpartmc~t of Environment, Hc.alth, & Nawn.I Ruources Solid Wan.e Management Divi,ion SMIPLE Ai'IALYSIS REQUEST St.ate LabonilOry of Public Health P.O. Box 28047, 306 N. Wilmington St. Raleiyh, North C1ro!U11 27611-8047 lite Number ~tJ~t~o~0~O~L ~l,~o~tJ-&~a_s-z.~O __ Sample ID Numl CD-016-SD 08/12/98 1200 GRAB ! 12345678 CD081098, NC D. WILSON l(ameofSite Crf-.sf!' X Drum .'S>lec iteLoc;ition ___ Q,,,__,.J"-+,fo-"-','"-c;"')'--__ 7 ,,_, _,./ll _ _,C-=c• ___ Date Collected Collected By_ ORG-CLP VOA Sediment 54 D\gency: Hazardous W a.ste --Solid Waste Duperfund TCLP Compounds -- Sample Type Inorganic Compounds Results(mg/1) D Environmental Concentrate Comments -arsenic f!c6u luyv:.---barium Ground Water(]) Solid (5) -cadmium --E_ {,,,<i\tv+t1-,-,1,,I,/ (1/Nfr ,r----chromium . Surface Water (2) Liquid (6) -lead - &_(-;;,.fkc:lCd__ -mercury m-Soil (3) ' . Sludge (7) selenium ..... --. . . I . silver . " - -Other (4) ,; -Other (8) - f - -Organic Chemistry Inorganic Chemistry - r0et'cr Results (mg/I) Parameter Results(mg/l)(mg/kg) Organic Compounds Resuits(i11g/l) _ P&T:GC/MS -antimony -be=ne Acid:B/N Ext. arsenic carbon tetrachloride ---t_-· 2,4-D r_ ..... .. -·-···· barium -·-·-·---· ------·-·-·-·-··--· chlordane ---·-·-· -·-·-··-· --~--------· 2,4,5-TIJ.(Silvex) -beryllium -chlorobenzene chlordane ~ -cadmium -chloroform - I= heptachlor . -chloride o-cresol - hexachlor.oben.zene -chromium -m-cresol hexachlo r0 bu tad i enc cobalt . p-creso! -·," -- endrin copper cresol F --lindane :,1,., -fluoride 1,4-dichlorobcnzene - methoxychl or iron 1,2-dichloroethane --toxaphene lead 1, 1-dichloroethylene -- I: -manganese -2, 4-dichloroethy lene -mercury -heptachlor nickel hexacWorobenzene ---1--nitrate hexachlorobutadiene - selenium ~ hexacWoroethane --silver methyl ethyl ketone --FOR LAB USE ONLY sulfates nitrobenz.ene - loate Received "f-/L/-9r-J/,5{.U{; - -thallium penta.chlorophenol - -vanadium pyridllle -zinc tetr:1chloroethylene --.Date Extracted -pH -trichloroethylene -conductivity -2 ,4,5-trichlorophenol D:1te Analyzed 9:-I0-9§11d -TDS 2, 4, 6-trichl orophenol - .Reported By -flash point -vinyl chloride --endrin lindane -- Date Reported • methoxychlor -- 11..,b Number 982645 --toxaphen~ 2,4-D -- --2,4,5-TP (Silvcx) I OHS 3191 (Revised !'2193) I I NC Department oi Environment, Hulth, & Narunl Re1>ources SAJ\,IPLE Ai'IALYSIS REQUEST State l..a,bontory of Public Health P.O. Box 18047, 306 N. Wilmington St. Solid Wute Management Divi,ion Raleiyh.' North Carolina 27611-1'.047 11,iteNumber rev Ov / fR 'Q {o ::(5":n Sample ID Nm C0"016·SD 08/12/98 1200 GRAB 12345678 CD081098, NC D. WILSON ( ameofSite Cr(sfl'v l)cu~ ,~4;:.cal!ecte<lBy ,;J ./ -· -ORG-CLP EXT /PCB Sediment i te Loc.ition _,V"-"'-'l-"T-"7fv,.,J r,'-"1C!-;f-+--~/l)'-"-.;{_.-:c.. ___ Date Collected_ 55 tgency: __ Hazardous Waste __ Solid Waste ~fund TCLP Compounds Sample Type u Environmental Ground Water(]) IL Surface Water (2) m-Soil (3) ,,, ✓ Other (4) Concentr""Jte -Solid (5) -Liquid (6) -Sludge (7) -Other (8) Comments P'2..,iJDf e_,e/..,,/J'I_ . vWk,i,;1,,r{1L c",:6 cv1 '.::,1'0 !l ,.cc,{,,;' J. , t'------,------, Organic Chemistry Inorganic Chemistry IParameter Results (mg/I) . Parameter ResuJts(mg/l)(mg/kg) _ P§:T:GC/MS _J/2cid:B/N Ext. I ._ 2,4-D ." 2,4,5-TP(Silvex) chlordane hexachlorobenzene ----·----- ------I beptachlor hexachlqrobutadiene ------endrin .. I lindani: .;,. _ metho:iychlor _ toxaphene I~ PCB 5 <::o,/offm t- FOR LAB USE ONLY I Date R.,;,eived ;?--N -7r]/;q uJ b ~13-'W~~ • Date ExtractedfC,Bs-~-,;;,,6-LJ/f'VP "PcB'~ y-31-11i/P. Date Analyzed AJJM-,).r/-9 JlA J I Reported By Date Reported _________ _ I Lab Number 982(,46 I OHS 3191 (Revi:;eJ l~.'93) - antimony arsenic barium beryllium cadmium chloride chromium cobalt copper fluoride iron lead manganese ______ _ mercur; nickel nitrate selenium silver sulfates thallium vanadium zinc -pH conductivity ------- TDS flash r.oint Inorganic Com pounds Results(mg/1) arseruc -barium -cadmium -chromium -lead - -mercury selenium -silver - - - - Organic Compounds Results(mg/1) benzene - -carbqn tetrachloride chlordane --··-·- chJorobenzene -chloroform -o-cresol -m-cresol - -p-cresol cresol - -l ,4-dichlorobenzene 1,2-dichloroethane - -1, 1-dichloroethylene -2, 4-dichloroethylene -beptachlor hexachlorobenzene -hexachlorobutadiene -.... hexachloroethane -_ methyl ethyl ketone nitrobenzene - -pentachlorophenol -pyridine -tetrachloroeth y lene -trichloroethylene -2,4,5-trichlorophenol -2, 4, 6-trichla ropheno I -vinyl chloride endrin -lindane - -methoxychlor -toxaphene -2,4-D -2,4,5-TP (Silvex) I NC Department of Environment, Hc.alth, & Narural Ruourccs SAivIPLE Ai'l'ALYSIS REQUEST SLAte L&h6ratory of Public Health P.O. Box 18047, 306 N. Wilmington St. Solid W,"te Management Divi,ion Raleigh, North ~•rolina 27611-8047 liteNumber Alto 00 I lo0& a s-O SamplelDNumb, C0-017-SL 08/12/98 11 4o GRAB 1 12345678 CD081098, HC D. WILSON lfameofSite Cn·.sfl' x [),/,(m. ,5/-/e, Collected By . SOIL So•l I -. ORG-ClP VOA • S 7 SiteLocation_..,&_....._x_/o=~'·~/.~---,/1-' ~N-~C---~ __ DateCollecte<l ____ --;:======::..:..":=::":=======--. ige~cy: Haurdous W a.ste D Sample Type Environmental Concentrate Ground Water (1) Surface Water (2) Solid (5) Liquid (6) Solid Waste E-Soil (3) ,.,, 'i ' Other (4) ,.· Sludge (7) Other (8) Comments l---~---------'----, Organic Chemistry Inorganic Chemistry '... 1·Par:uner"er Result.5 (ing/1) f,, 1--1::::'P&T:GC/MS Acid:B/N Ext. 2 4-D ---2:4,5-TP(Silvcx) -·--·------···-·-.. -· ' -chlordan~ _ hep1'1chJor hexachlorobea.zene _____ _ _ hexachJo·r~bul'1d1ene~----- endri.n I = lindane •;: _ melhoxychlor -toxaphene 1 - - -I - I FOR LAB USE ONL y Date Received 1[-·/</-1('VJJ /,t/6 _ ✓ I Dale. Extracted _________ ~ Date Analyzed ~9_-~L~0_-~9~6~n~2- • Reported By 1 Date Reported Lab Number I OHS 3191 {Revi5ed l-:..'93) 982647 Par:uneter Result.s(mg/l)(mg/kg) antimony arsenic barium -. beryllium - - - cadmium chloride chromiu:n cobalt copper fluoride iron lead manganese mercury nickel nitrate selenium silver sulfates thallium vanadium zinc pH conductivity~------ TDS fl~h point TCLP Compounds Inorganic Compounds Result.s(mg/1) arseruc -barium· ----------- cadmium -chromium -!e-"d - -mercury selenium -silv.er - ------------------ Organic Compounds benzene - carbon ttlrachioride .:h!mda.ne chlar::,benzene chloroform a .. cresol CJ.--<:resol p_.-crcsol creso\ 1,4-dichlorobenz.eae _ 1,2-dichlorodhane Result.s(mg/\) _ l, 1-dichloroethylene ______ _ _ 2,4-dichloroethylene ______ _ _ bep1'1chlor hexachlorobenzene hexachlorobutadiene _______ _ -.. hexachloroethan::: -__ methyl ethyl ketone nitrobenzene - -pe:1ta~hlorophenol -pyridine -tetrachloroethy Jene -trichloroethyiene -2, 4,5-trichlorophenol -2 ,4,6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphene -2,4-D -2,4,5-TP (Silvex) - I NC Department of Environment, Hulth, & Natural Rc,our·ccs SAi'vIPLE Ai'IALYSIS REQUEST Slate Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Solid Wuu: Management Diviiion Raleii,:h, North Carolina 27611-8047 lliteNumber fi!t:v Oo I /p D lo ,::? z:;:n Sample ID Numbe C0-017-SL 08/12/98 1140 GRAB . . 12345678 CD08!098, NC O. WILSON (ameofSite ~iteLocation C,(sf/'v V -1/4,~ l)cu tn ':S:4; ,Collected By_ SOIL ~ ORG-CLP EXT /PCB Soil /IJ [_,,-DateCollected 58 n,gency: Hazardous Waste Solid Waste ~fund TCLP Compounds ---- D Sample Type Inorganic Compounds Results(mg/1) EnvironmenL1I Concentrate Comments -arseruc barium -Ground Water (I) -Solid (5) -cadmium E_ -chromium Surface. Water (2) -Liquid (6) -lead ~Soil (3). -mercury Sludge (7) I • -se.enium -silver - -Other.(1) -Other (8) - I - -Organic Chemistry Inorganic Chemistry - 'Parameter Results (mg/I) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) . ~T:GC/MS antimony benzene --_ Acid:B/N Ext. arseruc carbon tetrachloride --I 2.4-D barium chlordane ---------·-· , -· ---···---· -· -··-" -· ---· -·--·-·-·-- _ 2,4,5-TP(S,lvex) -beryllium -chlorobenzene 1 chlordane cadmium chloroform --heptachlor . chloride o-cresol , --_ .hexachlorobe:izene -chromium -m-cresol I _ hexac~orobutadiene -cobalt p-cresol - endrin copper cresol --I lindane• fluoride 1 ,4-dichlorobenzene --_ methoxychlor iron 1,2-dichloroethane --toxaphene lead I, 1-dichloroethylene I l_k: :;(l~ --e_e, 13. I), l/-¥Dhf. -manganese -2, 4-dichloroethylene , heptachlor -mercur; -nickel hexachlorobenzene ---•t--nitrate hexachlorobutadiene -selenium ~ hexachloroethane --silver methyl ethyl ketone --FOR LAB USE ONLY sulfates nitroberuene I Date Received 'i?-/(/-Cj 'iY(; 1,,/t; -- -thallium pentachlorophenol - --vanadium pyridine . -tl\A 0-)0C\6,,_.n -zinc tetrachloroeth :1 I ene -I Date ExtractedfeBi y-,;J. 7-'f_WP -pH -trichloroethylene 'P~ z.-31-98VP -conductivity -2, 4,5-trichlorophenol Date Analyzed AAl,4~.:l</--9Pti{J -TDS 2, 4,6-trichlorophenol -I Reported By -flash point -vinyl chloride --endrin lindane --Date Reported --methoxychlor I '--1~ Number 982648 --toxaphene 2,4-D · -- --2,4,5-TP (Silvex) I OHS 3191 (Ri:vi5cJ 11/93) I NC Dcp1.rtmcn! of Enviroruncnt, Hullh, & Nawral Re&ourccs SAl\i1PLE Al'l'AL YSIS REQUEST SlAte Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Solid Wut.c Maru.gcmcm Divi,ion Ralei~h. North Carolina 2761 l-8047 . liteNurnbcr Nto OD I lo!Jlt a s-O SampldD Numb, C0-018-SL 08/13/98 1405 GRAB larrieofSite Cn·s f,,, X l) /IA 111 :i/lc, • 12345678 CDO81O98, NC D. WILSON Collected By_' SOIL Site Lm:;it ion ___ t).;,_.,,_x,.__,_!o_,,_,'--~{J~----+'--'N-·...,e--"'·---Date Co llecte<l I ' ORG-CLP Bgency: Hauirdou.s Waste Solid Waste Sample Type D Environmental Concentrate Comments Ground Water (1) -Solid (5) Surfac7 Water (2) -Liquid (6) Il-Soil (3)' •, Other (4) ', --Sludge (7) -Other (8) l---~--- Organic Chemistry Inorganic Chemistry f ar~et'er · I _V_P P,&T:GC/MS Acid: BIN Ext. F ·2,4-D, 2,4,5-TP(Sdvex) chlordane heptachlor hexachlorobenz.ene R~ults (mg/I) ------ -hexactiJ?ro!JUtadiene ______ _ endrin ·i_ I lindai1e· : j _ methoxychlor F tox~phene . I FOR LAB USE ONL y ~ate Received ?,-/ L/-9' ?J//J 11/6 tate Extracted _________ _ Date Analyzed _..:_<1_-I_O_-C/..:..c..6_'/ly..:... '-=-- .Reported By .Date Reported Lab Number, --~9:,,. .. c,:Sw'?"",6'-'-'=4.,.,9,.,__ IDHS 319) (Rcvi5cd 12/93) Parameter Results(mg/1) (mg/kg) -antirr.ony arsenic -barium -·-··· --·-···---·-·-··---···- -beryllium cadmium -chloride -chromium -cobalt - -copper fluoride --iron -lead - -manganese -mercury nickel -nitrate -selenium -silver - sulfates -thallium - vanadium -zinc - -pH -conduc~iviry TDS - -flash point - - · VOA Soil 116 TCLP Compounds Inorganic Compounds Results(mg/1) arseruc -barium -cadmium -chromium -Je;id - -mercury selenium -silver - - -- - Organic Compounds Results(mg/1) benune -c:ubon tetrachloride -chlOrdane -·-·- chlorobenunc -chloroform -o-cre:ml -rn-cresol - -p-cre.sol cresol - -1,4-dichlorobenzene 1,2-dichloroethane - -1, 1-dichloroethylene -2, 4-dich!oroethylene -heptachlor hexachlorobenzene -hexachlorobutadiene -.... hexachloroetbane -_ methyl ethyl ketone nitrobenzene - -pentachloropbenol -pyridine -letrachloroethylene --· trichloroethylene -2, 4, 5-trichlorophenol -1, 4 ,6-trichlorophenol -vU1y\ chloride endrin -lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Silvcx) I NC Department of Environment, Hullh, & Narural Resources Solid Wute Management Divi,ion SAJYIPLE A.i'l"ALYSIS REQUEST SlAtc Laboratory of Public Hc:.allh P.O. Box 28047, 306 N. Wilmington St. RakiHh., North Carolina 27611·8047 lite Number /1/1; D OD j ip Q (o ::? r;-n Sample ID Number/i C0-018-SL 08/13/98 1405 GRAB 12345678 C0081098, NC O. WILSON ... ameofSite 1liteLoe..1tion Cr(sfl'y rDcr~ tn ,5;! _eouectedBy_· ·_ s01L / {f,. ORG-CLP EXT /PCB Soi J t) 'I :fvJ r~ /l/ l--. DateCollected ____ ======-----1-=1-7 __ _ tgency: Hazardous Waste Solid Waste ~fund Sample Type u Em·ironmental _ Ground Water(!) L Surface \'hter (2) f Soil (3) .: :_, _ Other (4)•:-. Concentr.:1te -Solid (5) -Liquid (6) -Sludge (7) -Other (8) Organic Chemistry l ' Parameter , _ P§:T:GC/MS ·. ~cid:B/N Ext. I· 2,4-D. ·= 2,4,5-TP(Silvex) chlordane· Re,;ults (mg/1) ------- heo. tachlor I hexachloroben.z.ene _____ _ hexach!Orobu tadiene •,·· ------endrin ._,. ' -!Lndane , { · _ methoxYchlor _ toxapheni.: 11...IL' PCB., ll=-------, FOR LAB USE ONLY IDate Received ?-/¥=:Wvews rv 6-24-<le>"'""" • Date ExtractcdPC8$'"3'.-;i.7-91VP. '1'C8~ 1{-:ll-9a'VP Dille Analyzed /WA:J'-2.-1--f·f',tJJJ I Reported By Date Reported _________ _ I Lab Number 982650 I DHS 319! (Revised l:2/93) Comments Inorganic Chemistry Parameter · Result.s(mg/l}(mg/kg) antimony - - - - arsenic barium beryllium cadmium chloride chromium cobalt copper fluoride iron lead .. manganese mercury nickel nitrate selenium silver sulfates thallium vanadium zinc pH conductivity ______ _ TDS flash point TCLP Compounds Inorganic Compounds Result.s(mg/1) arsenic -barium -cadmium -chromium -lead - -mercury selenium -silver - - - - Organic Compounds Results(mg/1) benzene -carbon tetrachloride -chlordane ---· chlorobenzene - chloroform -o-cresol -m-c:esol - -p-cresol cresol - -1,4-dichlorobenze□e 1,2-dichloroethane - -I, 1-dichloroethylene -2, 4-dichl o roetb y Jene -beptachlor hexachlorobenzene -hexachlorobutadiene -... hexachloroethane -_ methyl ethyl ketone nitrobenzene - -pentachlorophenol -pyridine -tetrach.!oroeth ylene -trichl0roethy lene -2, 4 ,5-trichlorophenol -2, 4, 6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphe□e -2,4-D -2,4,5-TP (Silvex) NC Department oi Environment, Health, & Natural Re1oources SAJVIPJ:_.E Ai'\'ALYSIS REQ1JEST SLl.tc Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Solid WuLe Muugcmcm Division Raleigh, North Carollfla 27611-8047 liteNumber It/to 00 I /oO& ol s-O Cn·sfl'x D,um 5>te, Sample ID Num C0-019-SL 08/13/98 1335 GRAB 12345678 CD081098, NC D. WILSON .-iameofSite '3iteLoC.1tion & , In r r:I N c,_ ' ' ! Collected By_ SOIL 0RG-CLP Date Collected - tgeocy: --Haurdous Waste Solid Waste _0uperfund -- Sample Type u Environmental Concentrate Comments -Ground Water (1) -Solid (5) IL Surface W,ater (2) -Liquid (6) II Soil (3) : ·:, -Sludge (7) Othe~ (4)}:' Other (8) --,. ~ Organic Chemistry Inorganic Chemistry ~P~r Results (mg/I) Parameter Results (m g/1) (mg/ kg) _ P&T:GC/MS -antimony -Acid:B/N Ext. -arseruc 2,4-D. ,. ·-·-·-·-·-·-·-·-· -· ·-····-·--·-·-·-barium -· = 2,4,5-TP(Silvex) -beryllium -chlordane• -cadmium heptachlor chloride -hexachlorobenzene chromium - a hexachlorobutadiene -cobalt endrin -copper lindane•.·.,rj. fluoride '•; -methoxy,chlor iron --toxaphene lead -I -manganese -mercury nickel --it-nitrate -selenjum -silver - FOR LAB USE ONLY sulfates - IDate Received ?-/~-'ff v'( o)G -thallium -vanadium zinc -I Date Extracted -pH 9-10-9011.t -conductivity Date Analyzed -TDS I Reported By -fb.sh point - -Date Reported - ILab Number 982651 - - -I OHS 319! (Revised 12193) VOA Soil 123 -· TCLP Compounds Inorganic Compounds Results(mg/1) arse::uc -barium -cadmium -chromium. -lead - -mercury sele!Uum -silver - - - - - Qrganic Compounds Results(mg/1) benzene -carbon tetrachloride -chlordane -·----chlorobenzene -chloroform -o-cresol -m-cresol - -p-cresol cresol - -1,4-dichlorobenzeoe -1,2-dichloroetha.ne -1, 1-dichloroethylene -2, 4-dichlo roe thy I ene -heptachlor hexachloroben.zene -bexachlorobutadiene - ' hexachloroetbane - -methyl ethyl ketone nitrobenz.ene - -pentachloropbenol -pyridine -tetrachloroethylene -trich]oroethy lene -2, 4,5-trich]orophenol -2, 4 ,6-trichlorophcnol -· vlnyl chloride endrin -lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Si!vex) I NC Department oi Environment, Heallh, & NaOJn.l Resources SAivIPLE Ai'IALYSIS REQUEST SlAtc Labomory of Public Hu!th P.O. Box 28047, 306 N. Wilmin!,,>tOn St. Solid Wut.e Management Diviiion Raldi;h.' North C1.ro!in127611-8047 liteNumber /i/C:1 Ov / & D (o:? s=o Sample ID Numb, C0-019-SL 08/13/98 1335 GRAB I.L A-12345678 CD081098, NC 0, WILSON C -_L 7'-. -<:.f. SOIL rameofSite ~r(SJl'Y rf,)Ct1 tr/ 1 41(, _Collecte<IBy_ ORG-CLP EXT/PCB Soil Siteu,c1tion ~()~-~'l~·fr;,..,_,__r;_.,~.f-~--r-~/I)'-'{_,.-=--· ___ DateCollected ____ -;::::======---==--l-2_4 ___ _ lgency: __ Ha=dous Waste __ Solid Waste ~fund Sample Type II Environmental Ground Water (I) r· Surface Water (2) Ir Other (4).' n Concentrate -Solid (5) -Liquid (6) -Sludge (7) -Other (8) u Organic Chemistry i('"ararneter IF' P&T:GCIMS -~,d:B/N Ext. Results (mg/I) r ,.D -I[_:: ;:;:5-~(Silvex) ------------ chiordan'e · II--hept.ichlor (L_ hexachlorobenzene _____ _ _ hexachlor9,butadiene~----- I= en<lrin · · · li~'dane ; __ : ~ _ methox)'.dilor toxapheile p PCS\ 1-- I FOR LAB USE ONL y Date Receive,! ~/f-'lf"f/e-oJG ~15-24.-CffyUY'\ • Date Extracted Pe8s f'.-27-9'1:IIP 'Pt!Bfs-~-3/-9~-VfJ - Date An:tlyze<1.Aµ,43,2,f-9K(J,P IReporte<I By - .Date Reporte<I Lab Number 982652 IDHS 319] (Rcviml l~/93) Comments Inorganic Chemistry Parameter Results(mg/l)(mglkg) -antimony arsenic -barium ·---·--·-· -beryllium cadmium -chloride -chromium -cobalt - -copper fluoride -iron - lead - -manganese -mercury nickel -nitrate -selenium -silver -sulfates - thallium -vanadium - ZlilC - -pH -conductivity TDS - -flash point - - - - - - TCLP Compounds Inorganic Compowuls Results(mg/1) arsenic -barium -cadmium -chromium -lead - -mercury selenium -silver - Organic Compounds Results(mg/1) benzene -carbon tetr.icWoride -chlordane -·-· chlorobenune -ch..loroforrn -o-cresol --------m--cresol - -p-cresol cresol - -1,4-dichlorobenzene 1,2-dichloroethane - -1, 1-dichloroethylene -2, 4-dichloroethy Jene -bept.ichlor hexachloroben.zene -hexachlorobutadiene -..._ hexachloroetbane -_ methyl ethyl ketone nitrobenzene - -pentachloropbi.:nol -pyridine -tetrachloroethy lene -trichloroethy lene -2 ,4,5-trichlorophenol -2, 4,6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphene 2,4-D -- -2,4,5-TP (Silvex) I NC Dep1r1ment of Environment, Health, & Narur:al R~ourccs -Solid Wuu: Maru.gcmcnt Divi,ion SAivll'LE Ai~ALYSIS REQUEST St.a.cc Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Raleil!h, North Carolina 27611-8047 llsite Number ..,A!"'--"<tC-'o'-<--"'0-'0"--'-/-'-'lo~rJ~(~e_,~'-'-_,SL'--0 __ Sample ID Numb, C0-021-SL 08/13/98 1500 GRAB 12345678 C0081098, NC 0. WILSON NameofSite C,--,·.sfl'x JJr{,(m ,2i1c, CollectedBy_S0IL I 0RG-CLP VOA Soil SiteLoc:ition _ _.[J_,,...__,x~lo~~r~//~--7-;-'-'N-~e-=· ___ DateCollected_ 64 tgency: Haurdous Waste Solid Waste TCLP Compounds Sample Type 0 Environmental Concentr.ite --Ground Water (!) -Solid (5) n_ Surface '!'later (2) -Liquid (6) ~ Soil (3)• ,. -Sludge (7) Other (4)_~,, Other (8) I -- ,.:. Organic Chemistry ' Paran,)etl!r ..Jc:::"P&T:GC/MS Acid:B/N Ext. Results (mg/I) 2,4-D. j, 2,4,5-TP(Silvex) -chlordane! hept:ichlor ,--- hexachlorobenz.ene ------.1,-~ -i1eXa~~1o;rt~,butadiene~----- endnn · .. ; I. ,l, , •• .,•,, tnu.<\Ili! \_:.~ -4[_·. rnethaxycJtlor I_ -toxapht:ne. I= 1=--------l FOR LAB USE ONLY I Date Received 5?-/q-yy(/,4' OJG, I Date Extracted . Date Analyzed t:j'-//-q'i( 1/d I Reported By Date Reoorted I Lab Nu~ber __ 9_8_2_6_5_3 __ - I DHS 3191 (Rcv;,cd lC:93) Comments Inorganic Chemistry Parameter Results(mg/l)(mg/kg) -anlimony arsenic -barium ---··----··. . ·-·--··--· -beryllium cadmium -· chloride -chromium - cobalt - -copper fluoride -iron -lead - -manganese -mercury nickel -nitrate - selenium -silver -sulfates -thallium -vanadium -zinc - -pH -conductivity TDS - -flash point - Inorganic Compounds Rcsults(mg/1) arseruc -barium -cadmium -chromium -le:id - -mercury selenium -silver - - - - ·organic Compounds Results(:ngl!) benzene -carbon tetrachloride -chlordane ---·- chlorcbell.Ztne -chlorofonn - o-cresol -m-cresol - -p-cresol cresol -1,4-dichJorobenzene -1,2-dichloroethane - -I, 1-dichloroethylene -2, 4-dich lo coelh y I ene -heptachJor hexachlorobenzene -hexachlorobutadiene -... bexachloroetha.ne -_ methyl ethyl ketone nitrobenzene - -pentachloropbenol -pyridine -tetrachloroethylene -trichloroethylene -2 ,4,5-trichlorophenol -2, 4 ,6-trichlorophenol -vinyl chloride endrin - lindane - -methoxychlor -toxaphene -2,4-D -2,4,5-TP (Silvex) I NC Department of Environment, Hullh, & Nawral Re1oourccs I Solid w .. ., Muugcmcnt Division· SAJ'vIPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 18047, 306 N. Wilmington St. Rakigh_, North Carolina 27611-8047 GO lo (;? r:;:n Sample ID Nuc C0-021-SL 08/13/98 1500 GRAB . ~ :/.. 12345678 CD081098, NC O. WILSON ]) ru In ,5, i & .Collected By_ SOIL -ORG-CLP EXT /PCB Soil r, I /' {.!L C...--Date Collected 6 5 - SiteNumber fil(D Ov I ltameofSite C,(sfl'y SiteLoc:1tion t) '{(vcd; lgeocy: H=dous Waste Solid Wa.ste ~fund TCLP Compounds ---- g Sample Type Inorganic Compounds Results(mg/1) Environment.al Concentrate Comments arseruc -barium -n--Ground Water (1) Solid (5) --cadmium ---chromium Scrface Water (2) Liquid (6) lead -- 0-(soil (;) · -'; -mercury Sludge (7) selenium --silver ' -Other.(4):' -Other (8) -~----- Organic Chemistry Inorganic Chemistry - tParameter Results (mg/I) Parameter Results(mg/1) (mg/kg) Orga11ic Compounds Results(mg/1) . ~T:GC/MS -antimony -benzene 11:-~ctd:B'.N Ext. arsenic -carbon tetrachloride -.,4-D ... , .. , barium chlordane -2,4,5-TP(Silvex) ------·--•---·-·---··-·--• -·-----·-------· -· -·-· -·--.-·--. -·-·-·---.. beryllium cblorobenzene -. -chlordane.'· --cadmium chloroform --beptachlor chloride -o-cresol -chromium m-cresol --he_xaC:hlOr.obutadiene cobalt p-cresol -- endrin copper cresol -- lmdane , -fluoride -1,4-dichlorobenzene ~ = melhoxychlor -iron -1,2-dichloroethane _ toxaphene -lead -1, 1-dichloroethylene ....k'.:" e. C. B. :i < 0,/0jp'\ -manganese -2, 4-d ichlo roe thy lene --mercur; -heptachlor -nickel -hexachlorobenzene nitrate hexachlorobutadiene -- I selenium ' hexachloroethane --silver methyl ethyl ketone I --FOR LAB USE ONLY -sulfates nitrobenzene - Date Received 'fr-/1,t'-95't/l;{)K;, -thallium penLachloropbenol -vanadium pyridine I ~-8-24-«e-dn --zinc tetrachloroethylene Date Ext;acled,.Pr1,l,i ')T-:;l-7-n\/P -- -pH -trichloroethylene "Pe.s's 11-3/-9?1/P · -conductivity -2, 4,5-trichlorophenol I Date Analyzed l!W48'.-.2S-fie& TDS 2, 4 ,6-trichlorophenol -- -flash point -vinyl chloride Reported By --endrin lindane --I Date Reported --methoxychlor 982654 --toxaphene Lab Number 2,4,D --I OHS 3191 {R~vimJ 1:2/93) --2,4,5-TP (Silvex) I NC Departmcn! of Environment, Hcallh, & Natural Ruourccs Solid Wane Management Divi,ion SAl\'IPLE Ai'l"ALYSIS REQUEST SLa.te Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Ralei~h, North C.1rolU1a 27611·8047 r' . ,ite Number ,/IJ"-"'t'-'(""'-)_0"'-"O'-'-/ --'/,"'-o"-0->,/p'-"'o/'-Sc=-0 __ Sample ID N um, CD-022-SL 08/11/98 1340 GRAB -12345678 CD081098, NC D. WILSON - - -'-'-' -__,_ -ORG-CLP VOA Soil l ameofSite Cn·,5fl'x D,u,y, ,Sile, Co!lectedBy:_ SOIL iteLoc:ition _,,.,Q.._,,.,'X_,,_fn=.-~/'.~/ __ 7+-,~/ll-~~~--DateCollected ____ -;=======.:·:,· :-===·=6=7====::,,., Hazardous Waste Solid Waste 0uperfund Sample Type II Environmental Concentrate Comments Grouod Water(!) -Solid (5) L Surface Water (2) •' -Liquid (6) Soil (3) ,·\· -Sludge (7) ' Other (4) ➔i ! -Other (8) Organic Chemistry i;:,Paranyrer '· t. VP&T:GC/MS ~,i _ Acid: BIN, Ext. Results (mg/I) ' ··-~:::~ Jisiivex) ---· -' ' -------chlord:ine J, · _____ _ heptachlor '. . hexachlor9benzene ------ hcxachlorObutadiene ~-----endrin t I I I l- lindanei~,1t: methoxycf\l,or toxapht!ne FOR LAB USE ONLY IDate Received <j{'--/~-'7V'(/~v/6 ., I Date Extracted Date Analyzed __ q~-~/ /_-_Cj~f~1/~,~2- • Reported By Date Reported _________ _ I Lab Number S82655· I OHS Jt9t (Revised 12193) Inorganic Chemistry Parameter Result.s(,ng/l)(mg/kg) antimony - - - arsenic barium beryllium cadmium chloride chromium cobalt copper fluoride iron lead m:lilganese ______ _ mercury nickel nitrate selenium silver sulfates thallium vanadium zrnc pH conductivity ______ _ TDS flash point TCLP Compounds · Inorganic Compounds arseruc -barium -cadmium -chromium -le.,d - -mercury selenium -silver - Organic Compounds benzene c~bon tetrachloride: - chlordane Result.s(mg/1) Result.s(mg/1) ... ,. . . -----·------.-. ·-·-.. ··--. c~orobenu:ie -chloroform -o-cresol - m-cresol - -p-c:esol cresol - -1,4-dichlorobcnzene -1,2-dichloroethane -1, 1-dichloroethylene -2 ,4-di chi o roetby I ene -hepiachlor hexachloroben.zene -hexa.chlorobutadiene -... hexachloroethane - _ methyl ethyl ketone nitroben.zene - -pentachlorophenol -pyridUle -tetrachlorc:!thylene -trichloroeth y lene -2 ,4,5-trichlorophenol -2,4 ,6-trichlorophenol -vinyl chloride endrin -lindane - -rnethoxychlor -toxaphene 2,4-D - -2,4,5-TP (Silvex) ~;~_ . -'~ ,. 't-' NC Dep1rtmcn1 of Environment, SAMPLE Ai'IAL YSIS REQUEST State Labora1.ory of Public He.Ith I Hc.ah.h., & N.1tural RC.!iource, P.O. Box 28047, 306 N. Wilminb'10n St. Solid Wut.c Muagcrrient Divi,ion Rall!ii:h, North Carolina 27611-8047 liteNumber ftltv Oo / {p Q (o « r:;:n Sample!DNum~ CD-022-SL 08/11/98 1340 GRAB . ..J_ . . . . • 12345678 CD081098, NC D. WILSON (ameofSite Site Location Cr(sfl'Y rDcu tn ,S:f .Collected By_ sort / ~ {£. ORG-CLP V 'lfvecr) /I)(__ DateCollected_· __ _ EXT/PCB Soil 68 .gency: __ Hazardous Waste __ Solid Waste ~fund TCLP Compounds Sample Type II Environmental CoTlcentrate Comments. Inorganic Compowuls -arseruc barium Results(mg/1) - Ground Water(]) -Solid (5) -cadmium chromium - Surface ,Yater (2) -Liquid (6) -le~d ~Soil (3) ;, _ Other (4).., -Sludge (7) -Other (8) -mercury I • -se.eruum silver - -11---'---r, ---,--------, Organic Chemistry Inorganic Chemistry - - - I 11 Parameter Results (mg/I) Parameter Resul ls(mg/1) (mg/kg) Organic Compounds Resulls(mg/1) I _ P_§cT:GC/MS ~cid:B/N Ext. 1--·-2,4-D ·.i,:: 2,4,5-TP(Silvex) chlordane ·' beptachlor. hexachlOroben.zene ------II= hexachlorobutadiene • l•_i. ~----- 11 -_ endnn .. ,. lindane .. , _ methoxyS'fllor _ toxaphene I _..J.c' PCB 5 -'=----FOR LAB USE ONLY I Date Received j"-/L/-r?Jlf; t?,/6 ~ 6-24-"!e.c.,Y\ I Date Extracted PC8; '?-;;Zl-17Yf' 7'CB~ ?-3t-9YVP Date Analyzed i;AJIH?--2.S--9 S'.4() I Reported By Date Reported I Lab Number __ 9_8_2_6_5_6 __ - - - antimony arsenic barium beryllium cadmium chloride chromium cobalt copper fluoride iron lead manganese ______ _ mercury nickel nitrate selenium silver sulfates thallium vanadium zinc pH conductivity_· ______ _ TDS flash point benzene -carbon tetrachloride - chlordane -·-·-. chJorobenzene -cWoroform -o-cresol -m-cresol --p-cresol cresol - -1,4-dichlorobenze□e 1,2-dichloroethane - -l, l-dichloroethylene -2, 4-dichloroethylene -heptachlor . hexachlorobenzene -hexachlorobutadiene -... hexachloroetbane -. _ methyl ethyl ketone nitrobenzene - -penl:achlorophenol -pyridine -tetrachloroethylene -trichloroethylene -2, 4,5-trichlorophenol -2 ,4 ,6-trichloropheno! -vinyl chloride endrin - lindane - -methoxychlor -toxaphene -2,4-D -2,4,5-TP (Silvex) I NC Department of Environment, He.allh, & Nao.iral Ruources SMIPLE Ai~AL YSIS REQUEST St.Ate Laboratory of Public Health P.O. Box 18047, 306 N. Wilmington St. Raleii::h, North Cuolina 27611·8047 I Solid Wute Management Division SiteNumber Alto 00/ loOIP ol s-D SampldDNuu CD-023-SL 08/11/98 1410 GRAB · _ I 12345678 CD081098, NC D. WILSON INameofSite Cn·.sfl'x [),1,un ,2i7e, Col!ectedBy-1SOIL . I ORG-CLP Sitel.oe.1tion () X fo,·(. , /11 (--DateCollected ----</;,!.,;,e...~e.~/...U'..C-''"''------1f--'-''--'='C.----- .Agency: Hazardous Waste Solid Waste _0uperfund I Sample Type Environmental Concentrate .-Ground Water(!) -Solid (5) Surface Water (2) Liquid (6) -- " I-Soil (3) ,:'.\ -Sludge (7) ·I Other (8) -Other (4) • - Organic Chemistry Paral;)efer · _V_P P,&T:GC/MS Acid:B/N Ext. ____ 2,4-D j,. • _ •2,4,5-TP(Silvex) chlorda.i.!e / hcptachiar hexachlorobenzene Results (mg/I) ------- '= I )\,; ------ hcxachl~r;obutadiene _____ _ endriri ,;i.. lindane';} methox)i~hlor I toxaphene I ----------------~ D . FOR LAB USE ONL y Date Received ?-#-'J?ytu/6 D Date Extracted _________ ~ .Date Analyzed~ D Reported By m Date Reported Lab Number 982657 II DHS 3191 (Revised 12/93) Comments Inorganic Chemistry Parameter Results(mg/l)(mg/kg) - - antimony arsenic barium beryllium cadmium chloride chromium cobalt copper fluoride iron lead manganese ______ _ mercury nickel nitrate selenium silver sulfates thallium vanadium ZlnC pH conductivity ______ _ TDS flash point VOA Soil 70 TCLP Compounds Inorganic Compounds Results(mg/1) arseruc -barium -cadmium -chromium -ie.ld - -mercury I • se.eruum -silver - - - - ------- Organic Compounds Results(mg/1) be:izene -carbon tetrachloride .. - chlordane ' --··· ·--··---··--------chlorobenzene - chloroform -O·cresol - rn--cresol - -p-cresol cresol - -1,4-dichlorobenz.ene 1,2-dichloroethane - -I, 1-dichloroethylene -2, 4·dichloroethylene -beptachlor bexachlorobenzene -bexachlorobutadiene -~ hexachloroelhane - -methyl ethyl ketone nitrobenzene - -penta.cWoropbenol -pyridine -te~:-achlpro_ethyle:ie · -trichloroethy lene -2, 4,5-trichlorophenol -2, 4, 6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphene -2,4-D -2,4,5-TP (Silvex) . I NC Dep,rtm,nc oi Env;ronmonc, SAivIPLE Ai'IAL YSIS REQUEST Sc..co I.Aboc,cory of PubU, Hu]ch Hca\lh, &. Na.rural RC1iourccs P.O. Box 28047, 306 N. Wilmington St. Solid Wute M1rugcmcn1 Divi,ion Rall!ii;h, North Cuolin1 27611-8047 lsi~Number /ltv OD / fe Q (o ~ Z::CQ Sample!DNum' C0-023-SL 08/11/98 1410 GRAB C -_j_ 1) <'-f. , 12345678 C0081098, NC 0. WILSON • Name of Si~ _I( Sfl'Y r~Cu tY/ <,4.t.{, ,Collected By_ SOIL F\ ;J ./ 1/J /' ORG-CLP EXT /PCB Soil SiteLoc:,tion [./ x' fyj_r-47 _ L---Da~Collected 71 .Agency: --Hazardous Was~ --Solid Was~ ~fund TCLP Compounds Sample Type Inorgani.c Compounds Results(mg/1) I Environment.a.I Concentrate Comments -arsenic barium -Ground Water (!) Solid (5) -cadmium -- •-' chromium _,. -Surface Water (2) Liquid (6) -lead -a ✓ Soil (3) :.' -mercury Sludge (7) -selenium -silver - -Other (4);.:•: -Other (8) - I l - -Organic Chemistry Inorganic Chemistry - I Parameter· Results (mg/I) Par:uneter Results (mg/l)(m g/kg) Organic Compow1ds Results(mg/1) ~T:GC/MS antirr.ony benzene --·_ id:B/N Ext. carbon tetrachloride " arseruc -.- ' 2,4-J) ,,, . . . --·-· -b:i.ri11m chlordane .:_::_: 2,4,5-TP(Silvex) ··-. -·----·-·--··-·-· -· -·--··-·-· ---·-·-·-·-· ---·--··--·-·-·-·-·-··--·- -beryllium -chlorobenzene _ chlordane ,~ -cadmium -chloroform 1 heptachlor -chloride -o-cresol 1 _ ·hexachlo:obenzene chromium . m-cresol -- -hexach)or~but.adiene -cobalt p-cresol -endrin . '; coppec cresol I -' -- -lindane ·"', -fluoride -1,4-dichlorobenzene -methoxy'~hlor iron 1,2-dichloroethane tox:iphen~ -- --lead 1, 1-dichloroethylene - I ..1:::: [!_ L. 13. :i <o,/tJ~ -manganese -2, 4-dichloroetby Jene I beptachlor --mercurJ -nickel bexachlorobenzene --- I -nitrate hexachlorobutadiene --selenium ~ hexachloroethaoe --silver methyl ethyl ketone --FOR LAB USE ONLY sulfates nitrobenzene I Date Received Z-,///-fflfe '!JJ<!; -- -thallium pentachlorophenol - -vanadium pyridine -· tf,,f\.· 0-~ 46 L-(y\ . -zinc tetrachloroeth y l ene -I Date Extractedft!Rs Y--::z:7-"iJ'J!P -pH. -trichloroethylene -PeB:r ?-31-9!2f P. -conductivity -2, 4, 5-tri chi orophenol Date AnalyzedAI.J't9:~ ,?R,4, TDS 2, 4 ,6-trichlorophenol --I Reported By -flash point -vinyl chloride --endrin lindane --Date Reported --methoxychlor I Lib Number 982658 --toxaphene 2,4-D -- --2,4,5-TP (Silvex) I DHS 3191 (Revised 12/93) I NC Department of Environment, Hullh, & Nawral Re.rnurccs SMIPLE Al~AL YSIS REQUEST St.ate Labon.lOry of Public HCJ1.llh P.O. Box 28047, 306 N. Wilmington St. Raleil;lh, Nonh Carolina 27611-8047 I Solid Wut.e Management Diviliion Site Number ..... !J"'-"'t"-'o""--"'O-'D"-'-/-"'loc.,0'---'6.,_t1_,oi,::_:__cS-Z.,:_D __ Sample ID Nurnbe CD-024-SD 08/10/98 1628 GRAB · c 12345678 CD081098, NC D. WILSON t=eofSite {__ 7n·.5fl'x Drum ,5>-lec Site Loe.1tion _ _,.,t};,_,;c,X......,,_fo-'-'-','-'-("'j'-----,?f-' _,_/u_1 _.,,L,-"-• ___ Date Collected Collected By __ ORG-CLP .Agency: __ Hazardous Waste Solid Waste Duperfund I Sample Type Environmental Concentr.ite I-Ground Water (l) -Solid (5) -Surface :Water (2) -Liquid (6) II-Soil (3) .. Sludge (7) . ,( -·/ . ' [-Other ( 4) : · -Other (8) . Organic Chemistry -:.~ ii-'2 ~ Par~eter · .,(~ VP&T:GC/MS •;. _ Acid:B/_N Ext. ··--· 2,4-D•:\ · Results_ (mg/1) _ heptachlor I-2,4,5-Tp(Silvex) chlordarie ' ~ hexachlorobenzene hexa.chlof'~~butadiene"------- eadrin _____ _ 1mctane -•.. _____ _ l -methoxy'~hlor 1 _to_x_•_ph_e_n_e ________ _ I- ll= I FOR LAB USE ONL y . Date Received ?,--/./7-'7'.P'v(; W6 I Date Extracted _____ · ____ _ Cf-LL -5.8 '11.2 1 Date Analyzed Reported By I Date Reported 982659 Lab Number I DHS 319! {Ri:vised 11./93) Comments Inorganic Chemistry Parameter Rcsults(mg/l)(mg/kg) - - - - - - - - - - - antimony arseruc barium berJlliurn cadmium chloride chromium cobalt copper fluoride iron lead\ manganese------- mercury nickel nitrate selenium silver sulfates thallium vanadium 21nc pH conductivity ______ _ TDS flash point VOA Sediment 73 TCLP Compounds Inorganic Com pounds arsen1c barium - cadmium chromium lead mercury selenium silver Organic Compounds benzene - - - - - - - - - - - carbon tetrachloride chJord;ine chlorobenzene chloroform o-cresol ·m-cresol p_-cresol cresol 1,4-dichlorobenzene 1,2-dichloroethane l, 1-dichloroethylene 2, 4-dichloroetbylene beptachlor bexachlorobenzene bexachlorobutadiene ... hexachloroethane -_ methyl ethyl ketone nitrobenzene - -pt.:ntachlorophenol -pyridme -tetrachloroethylene -trichloroethy lt.:ne -2 ,4,5-trichlorophenol -2, 4, 6-trichlorophenol -vinyl chloride endrin -lmdane - -methoxychlor -loxaphene 2,4-D - -2,4,5-TP (Silvex) Rcsults(mg/1) Rcsults(mg/1) I NC Dcpartmcot· of Environment, Hullh, & Nawral Resources SAJ'vll'LE Ai'l"ALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Solid Wuu: Man.a2:cmcnt Divii;ion lite Number fi!Cn Oo I (e D (o ::? r:;:n Sample ID Number/, (ameofSile Cr[sfl'v ·,Dcu tr7 ,,5;7i _Collecte<lBy __ i te Loc.lti on __,,t)'-'x'."-'-fv-'-'-'-Ci-,c::i..i0'-. f-' -~/..:_/j--=(___=-___ Date Collected tgency: __ Hazardous Waste __ Solid Waste ~fund Sample Type I Environmental Concentrate L Ground Water(!) Surface Water (2) ' - - - - Solid (5) Liquid (6) Sludge (7) Other (8) Organic Chemistry Comments Inorganic Chemistry Raleii:h, North Carolina 27611-8047 CD-024-SO 08/10/98 1628 GRAB 12345678 C0081098, NC 0. WILSON ORG-CLP EXT/PCB Sediment 74 TCLP Compounds Inorganic Compounds Results(mg/1) arsenic -barium -cadmium -chromium -lead - -mercurj se!en.iurn -silver - ·~ I] Parameter ' · Results (mg/I) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) ,f~-P&T:GC/MS l>i ·~:d:WN Ext. ------- 0 ·,--2,4-D •:•' 2,4,5-TP(Silvex) chlordlli?-e " I-_ beptachlcir; hex:ichlorobcnzeae ------- 1 _ hexachlO_robutadiene ______ _ e~drin ·::, I= lindane .::· rnethaxy~°!Hor I -_ ., toxaphen·~ .~ Pt& s <12•'"ffm FOR LAB USE ONLY loate Receive<l?-//./-Wtfe t<lv e, I'-tr 0 -lA--9 6 \U'<\ I Date Extracted,A;Bj }7-;17-'17'/f 'PeBJ-'1-/-%1-VP Date Analyzed &.e?::8':-2-S"-'2 fA,lJ I Reported By Date Reported _________ _ I Lab Number 982660 ; I DHS 3191 (Rcvi~ed 11193) - - ---· - - - - - - - - - - - - - - - - - -- - - - -- - - - - - antimony -benzene arseruc carbon tetrachloride -barium chlordane ·-·-·-·-· _, beryllium -chlorobenzene cadmium chloroform -chloride o-cresol -chfomiurn m-cresol -cobalt -p-cresol copper -cresol fluoride -1,4-dichlorobenzene iron 1,2-dichloroethane -lead -I, 1-dichloroethylene manganese -2, 4-dichloroetbylene mercury -hept.achlor nickel hexachlorobenzene -nitrate bexachlo ro but.ad iene -selenium .._ hexachloroetbane -silver _ methyl ethyl ketone sulfates ' nitrobenzene -thallium -pentachlorophenol vanadium -pyridine ZlllC -tetrachloroethylene pH -trichloroethy lene conductivity -2,4,5-trichlorophenol TDS -2, 4, 6-tri chi o rophen ol flash point -vinyl chloride endrin - lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Silvex) I NC Department of Environment, HealLh, & Nawn] Ruourccs SMll'LE Ai'l'AL YSIS REQUEST St.ate Laboratory of Public Heallh P.O. Box 18047, 306 N. Wilmington St. Ralei!ih, North Carolina 27611-8047 I Sol;d w,.u, Muug,m,nt o;v;,;on SiteNumbcr Alto 00 I /oO(f as--D tamcofSite Cn·sfl'x Dru~ Si/4, Sample ID Nu, C0-025-SO 08/10/98 1620 GRAB 12345678 CD081098, NC D. WILSON SiteLoc:itioa ()_ X -fv rt'/ /II C-' lgcncy: ' I --H=irdous Waste Solid Waste _0uperfund TCLP Compounds -- Ccllected By ' -ORG·CLP Date Collected VOA Sediment 80 I Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comment'i arsenic -barium - t-Ground Water (I) Solid (5) cadmium , -- -chromium Surface "':'~ter (2) Liquid (6) lead --- I--mercury Soil (3) · . ! -Sludge (7) selenium - . ,, -silver Other (4) ;; · -Other (8) ,--, . - -Organic Chemistry Inorganic Chemistry -. rPar~r ' Results (mg/I) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) ~. -1:::_ P&T:GC/MS antimony ben.1.ene ·--- 1__ Acid:B!N Ext. arsen..1c carbon tetrachloride --___ · 2,4-D , .. barium chlordane ·-·--•-···•·--····-· ..... ·····-· . ··-··--·--·---.. ---.. ··-·-·---·-·· _ 2,4,5-TP(Silvex) -beryllium -chloroben.zene chlordatje I cad DU um chloroform j ·-- heptachJor -chloride o-cresol -hexachloroberu.ene chromium m-cresol , .. • -- hexach!0,t~ buta.diene -cobalt p-cresol ~- -endrin ,, copper cresol -- lindane •(~ · -fluoride 1,4-dichloroben.re□e - ' methoxychlor iron 1,2-dichloroethane -- toxaphene • lead 1, 1-dichloroethylene. -- -minganese -2, 4-dichloroelhylene ~ -mercury -heptachlor nickel hexachlorobenzene --nitrate hexachlorobutadie□e -- selenium ~ bexachloroethane -I -- -silver methyl ethyl ketone -I FOR LAB USE ONLY -sulfates nitrobenzene - Date Received ?--/f/-· 77J/t, u/6 thallium penLachlorophenol --vanadium pyridine --I Date Extracted -z.inc tetrachloroethy lene - -pH trichloroethylene - 9-11 ~ 9ft: 11 ✓ -conductivity -2, 4 ,5-trichJorophenol Date Analvz.ed -TDS 2,4, 6-trichJorophenol I Reported ~y - -flash point vinyl chloride - --endrin lindane --I Date Reported --methoxychlor 982661 --toxaphene Lab Number 2,4-D --I DHS 3191 (Revised 12/93) --2,4,5-TP (Silvex) I ' NC Department of Environment, Hu.Ith,&. Narural Ruourccs Solid Wut.c Management Divi,ion SMIPLE A.t'IALYSIS REQUEST SLB~c. Labor:atory of Public He.a!th P.O. Box 28047, 306 N. Wilmington Sl. Rakit:h, North Carolina 27611-8047 lsiteNumbcr /lltv Oo / & V (o ::; ,:;:n Sampl~ID Numbe: C0-02S-SO 08/10/98 1620 GRAB · 12345678 CD081098, NC 0. WILSON INameofSite Cr(sf17y rD_ru fY'. ,s;! ,Collected By_• ,_, 1.£, ORG·CLP EXT /PCB Sediment SiteLoc:ition~V~'/~frJ~,,-,...,~.,_~--/IJ~~(,_,_~ ___ DateCollected ____ -;:::======---===8=1===:...., .Agency: __ Hazardous Waste __ Solid Waste ~fund Sample Type I Environmental Ground Water (1) I_ Surface Water (2) 1-Soil (3) _:• 1 · ✓ Otiler (4)','. Concentrate -Solid (5) -Liquid (6) -Sludge (7) -Other (8) Organic Chemistry I Parameter P&T:GC/MS v,\cid:B/N Ext. __ .. 2,4-D , .. 2,4.5-TP(Silvcx) chlordane 1 bepuichlor Results (mg/I) hexachlorobenzene _____ _ hexachlorobutadiene endrin ;-·~-~----- lindane·:i;11, methoxychlor . . ' toxapnene -~~P~t"'-'--'Bc_,.s_ I- II FOR LAB USE ONL y I Date Received ~/£1-rr:ve (,Al G fl\.-1'-e ,'ZA-r qe, ~ I Date Extracted Pc8:f ;r-;J.7-'JirVP --PcB~ '9-l-9Y"VP . Date Analyzed M.4'i-2s•-9 rAzD I Reported By Date Repor1ed I Lab Number __ S_S_Z_G_G_Z_ I OHS 319! (Rcvi5cd 12/93) J:omments Inorganic Chemistry Parameter Results(mg/l)(mg/kg) - antimony arsenic barium beryllium cadmium chloride chromium cobalt copper fluoride iron lead manganese ______ _ mercury nickel nitrate selenium silver sulfates thallium vanadium zinc pH conductiviry ______ _ TDS flash point TCLP Compounds Ino~~an.ic Com pow1ds arsenic -barium -cadmium -chromium -lead - -mercury I • se,eruum -silver - Organic Compow1ds benzene carbon tetrachloride -chlordane Results(mg/1) Results(mg/1) -·-·-···-·-.. ····----......... ··-- chlorobenzenc -chloroform -o-cresol -m-cresol - -p-cresol cresol - -1,4-dichlorcbenzene -1,2-dichloroethane -1, l-dichJoroethylene -2, 4-dichloroethylene -bepl.ichlor hexachlorobenzene -hexachlorobutadiene -.._ hex.:i.chloroethane -_ methyl ethyl ketone nitrobenz.ene - -pentachloropbenol -pyridine -tetrachloroeth y l ene -trichloroethy lene -2, 4. 5-trichlorophenol -2, 4,6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -toxapherie 2,4-D - -2,4,5-TP (Silvex) I NC Department of Environment, Hc.allh, & Narural Resources SA.t-VIPLE Al'l"ALYSIS REQUEST StAce Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Solid W.ute Management Division Raleii::h. No~ Carolina 27611-8047 liteNumber /I/to OD I /o!J& a s-D Sample ID Numi C0-026-S0 08/10/98 1650 GRAS lame of Siu, SiteLootion Cn'.5fl'x Dru111 ,'Site, ' 12345678 C0081098' MC 0, WILSON Collected By_ Dai,,Collected , ORG-CLP YOA Sediment ()_ X Iv.-,/ N l--87 ( --- ' l lgeur.y: ---Haurdous W asu, --Solid Wasu, _Duperfund TCLP Compounds I Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments arsenic -bruiurn . - Ground W_ater (!) Solid (5) cadmium r -- -chromium Surface W~_ter (2) Liquid (6) Je;id --' mercury ' ' -1-Soil (3) -, Sludge (7) selellitim J)' --silver Other (4)1:> ---Other (8) - I , .. - I -Organic Chemistry Inorganic Chemistry I - , aran er t ' -1 ~:GC/MS Results (mg/I) Parameter Results(mg/1) (mg/kg) Organic Compounds Resu!ts(m;\i\) -antimony -benzene ,I_ Acid: !JIN Ext. arseruc carbo!l tetrachloride --1--2,4-D . barium chlordane . . .. ······-···--·--·-·-····· -·-•···· .. .--· ·-·---·-·-·-·---·····-·---·--· ------- 2,4,5-TP(Si!vex) -beryllium --chlorobenzenc 1= - chlonb.'rie -cadmium -chloroform -= heptachl~r, -chloride -o-cresol hexachlorobenzene chromium m-cresol ''r . -- ~ hexachloi"obut.ad iene cobalt p-cresol u~· --eridri.n I' copper cresol -- lindane ' fluoride 1,4-dichlorobenzene methoxy~tlor -- -iron 1,2-dichloroethane - ' toxaphene -lead I, 1-dichloroethylene ~- - -manganese -2, 4-dichloroethylene -mercury -heptachlor -nickel hexachlorobenzene -nitrate hexachlorobutadiene ---selenium ~ hexachloroelhane -- -silver methyl ethyl ketone -FOR LAB USE ONLY sulfates nitrobenz.ene .Dato Received ~~6 --thallium pent.achlorophenol -- -vanadium pyridine -zinc tetrachloroethylene -- .Date Extracted -pH -trichloroethy lene -conductivity 2, 4,5-trichlorophenol 9-//-9F 11d -Date Analyzed -TDS 2, 4 ,6-trichlorophenol -I Reported By -flash point -vU1yl chloride --endrin lindatie -- 1 Date Reported --methoxychlor 982663 --toxaphene Lab Number 2,4-D -- --2,4,5-TP (Silvex) OHS 3191 (Revised l 2!93) I NC Department of Environment, Hulth, & Nawral Re1,ourccs SA1V1PLE Ai'l"ALYSIS REQUEST StAtc Laboratory of Public Health P .0. Box 28047, 306 N. Wilmington St. Solid Wu~ Management Divi,ion Ralcii:h_, North Carolina 27611-8047 lsiteNumber /1/l;v Oo f fe D (o ::? ;;:n SampldDNuml C0-026-SO 08/10/98 1650 GRAB .Name of Site SiteLoc.1tion /1 -_j__ ,..., <:.f. 12345678 CD081098, NC D. WILSON Lr(sJI''{ ruo, tn •-41(, ,CollectedBy_: ;f\ JJ l /I) /' ORG·CLP V 'itvc(r) L----DateCo!lected__..! .Agency: Hazardous Waste __ Solid Waste -~fund Sample Type I Environmental .-Ground Water (1) Surface y,'.ater (2) 1-Soil (3): /other (4)'< Concentrate -Solid (5) -Liquid (6) -Sludge (7) -Other (8) Comments IJ---· ---,---------1 Organic Chemistry Inorganic Chemistry - 1.·~ 1 ._.'.1 Parameter ._ _ P~T:GC/MS ,; _0cid:B/N Ext. ., I -__ 2,4-D ; 2,4,5-TP(Silvex) chlordaiie "' Results (mg/I) I -_ hepLllchJor hexachlorobenzen_e _____ _ hexachl6robutadiene ~----- endrin , ' -lindane-,,i: = methoxyc_hlor _ toxaphene I~ PCB 5 I=-_ __ _ I FOR LAB USE ONLY Date Received <J?-/l/-<Jf11//;'WG . -.f>I\A\--o--24 c, e= I Date Extracted fCJ3s '/r;;;17:'J-rvf "?(!.[J's q-/-'13"1/P Date Analyzed 81,AU~'tfEhO I Reported By m Date Reported Lab Number II DHS 3191 (Revi.'icd 12/93) 982664 Parameter Results(mg/l)(mg/kg) - - antimony arsenic barium beryllium cadmium chloride chromium cobalt copper fluoride iron kad .•·-----·---,_, ____ manganese ______ _ i:nercury nickel nitrate selenium silver sulfates thallium vanadium Ztnc pH conductivity ______ _ TDS flash point ______ _ EXT/PCB Sediment 88 TCLP Compounds Inorganic Compounds arseruc -barium -cadmium -chromium -lead - -mercury selenium -silver - Organic Compounds benzene carbon tetrachloride -chlordane Results(mg/1) Results(mg/1) ---·-___ , __ ---·-----·--····-- ch..lorobenzene -chloroform -o-cresol - m-cresol - -p-cresol cresol - -1,4-dichlorobenzene 1,2-dichloroethane - -1, 1-dichloroethylene -2, 4-dichloroethy lene -heptachlor hexachlorobenzene - bexachlorobutadiene -~ hexachloroelhane -_ methyl ethyl ketone nitrobenzene - -penta.chloropbenol -pyridine -tetrachloroeth y l ene -trichloroethylene -2, 4,5-trichJorophenol -2, 4 ,6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphene -2,4-D -2,4,5-TP (Silvex) D NC Depu-tmcnt of Environment, H~lth, & Nawral Re.sources SAMPLE ANALYSIS REQUEST St.ate Laboratory of Public Health i;i.o. Box 28047, 306 N. Wilmington St. 1t,• . l' Solid Wut.c M1n.agcmcnt Divi,ion Raleit:h, North Carolina. 27611-8047 lliteNumber lilt O O O I lo O & ol ~o Sample ID Nurnt CD-033-SL 08/12/98 1545 GRAB ! 12345678 CD081098, NC D. WILSON lfameofSite SiteLocation Cn-.'Jfl'X JJ,11tn 121 :/c, CollectedB/_• SOIL 1 ORG-CLP U X /4,-f',/ / NL---DateCollected_c, --;,>'----,'"-/=~~----~--- VOA Soil 113 .gency: Hazardous Waste Solid Waste TCLP Compounds Sample Type II Environmental Ground Yfater (l) r Surface Water (2) \ t-Soil (3) :'.. · ,- Other (4(,. Concentrate -Solid (5) -Liquid (6) -Sludge (7) -Other (8) Comments 'fi+vol r_tx.t/11 GdYJ iaflt¼~ ;,,1 :,,?1..c<; fJe?1I e,L ' Inorganic Compounds arsen.1c -· - barium cadmium chromium le,d mercury selenium silver i J----'-, ----r-----'----1 _- Organic Chemistry Inorganic Chemistry Results (mg/i) Parameter Results(mg/l)(mg/kg) Results(mg/1) Results(mg/1) IPar:uyerer _V_P P&&T:GC/MS '· -~! .. ; 'f' Acid:B/N Ext. antimony arsen..ic Organic.Compounds ~nzene ~ban tetrachloride chlordane • beptachlor hexachJorobenzene ------ '.ti 1 1---;:::~-TP(Silvex) 1 _ hexachlorabutadiene~-----. . ' I= I I endnn ,.-, lindane ;;~· methoxyfhlor , loxaphene I FOR LAB USE ONLY Date Received ?-/~ · 7N /: Wb _,; I Date Extr~cted _________ _ Date Analyzed C/-llf--9'[ n:J I Reported By 1 Date Reported Lab Number I OHS 3191 (Revised ]'.2/93) 982665 - - - - - - - - - - - - - - - - - - - - - - - - - barium beryllium cadmium chloride chromium cobalt copper fluoride iron lead manganese mercury nickel nitrate selenium silver sulfates thallium vanadium zinc pH conductivity TDS -flash point chlordane -\/cl}loroben.ztne -U-hloroform o-cresol -rn-cresol _ p-cresol cresol -_vi ,4-dichlorobenzene ______ _ ....b::::"1,2-dichloroethane ~I, 1-dichloroethylene ______ _ _kC'2-;-4-d ich loroethy lene ______ _ _ beptachlor hexachloroberizene hexachlorobutadiene ... hexachloroetbane ~ethyl ethyl ketone nitrobenzene -_ pentachlorophenol _ pyridine _0etrach1oroethylene ~hloroethylene ------- _ 2,4,5-trichlorophenol ______ _ 2,4,6-trichJorophenol ______ _ ~tnyl chloride endrin lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Silvex) 0 NC Depan:menl of Environment, Health, & Nao.iral Rc.&ources SANIPLE Ai'IALYSIS REQUEST $LB.le Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Solid Wu~ Management Divi,ion Ral~ii;h_, North Carolina 27611-8047 0 U . / CD-033-SL 08/12/98 1545 GRAB llsiteNumber rvtv Ov / wD(o ~,:;-n Sample!DNu, 12345678 CD081098 NC D " SOIL ' · •llSON C,(sfl'y rD,c11 tr7 ,$4:; ,Collecte<l By' ORG-CLP EXT/PCB Soil rameofSite Sitelo□tion ~gency:. () ',( :fvJ r~ /IJ L--DateCollecte<l ___ ;::::=::=======---=-11:,:4:__ __ Solid Waste ~fund - Hazardo115 Waste Sample Type D Environmental Ground Water (1) D_Zrface -"".•ter (2) ~ Soil (3)_·•: Other (4)':i' Concentrate Commenti, -Solid (5) tl.'f-(21 c.t. ""J . -Liquid (6) c✓id-rt,,IAJ//4 ct] ' -Sludge (7) s✓c1uutvl:- -Other (8) ~-~-~---Organic Chemistry Inorganic Chemistry I'-\ 11 Parameter :_;: . _ PiT:GCIMS ~-:,'· I V'Acid:BIN Ext. ;; 2,4-D : 2,4,5-TP(Silvex) chlordane I-_ heptacWor hexachloroben.zene Results (mg/I) -------hexachl6'robutadiene d' 'i ~----- 1-_ er. nn ,:· lindane-·. _ methoxy~hlor I _ toxaphene 1~ PCB :Q:is¥J 1,J~fi'm 11- FOR LAB USE ONLY .Date Received 'ff-/1,L-:{E'{f WG fl'A g_ ltfl1 I Date Extracted PCl!J:f 1{,P?-Wf' -PCB's' L:f-l-9'$'VP. Date Analyzed LWA«-3/-9 IA 4> I Reporte<l By 1 Date Reporte<l Lab Number I Dils 3191 (Revised 12/93) 982666 Parameter Results(mg/l)(mg/kg) antimony arsenic b~rium beryllium cadmium -chloride chromium -cobalt -copper fluoride -iron -lead -. -mmganese -mercury nickel -nitrate -selenium -silver -sulfates - thallium - vanadium - Z.l□C - -pH -conductivity TDS - -flash point ... - - - - - - TCLP Compounds Inorganic Compounds Results(mg/1) arse:::uc -barium -cadmium -chromium -lead - -mercury selenium -silver - - - - Organic Compounds Results(mg/1) benzene carbon tetrachloride - ____ ., chlordane ---·------ chlaroben.zcne chloroform --t.L' o-cresol --1,.L m-cresol V p-cresol 0resol -1,4-dichlorobenzene ______ _ 1,2-dichloroethane - -1, 1-dichloroethylene -2, 4-dichloroetby Jene -heptachlor bexachlorobenzene -bexachlorobut.adiene - ~Woroethane yl ethyl ketone nitrobenzenc -pentachlorophenol -pyridU1e -tetrachloroethylene -trichloroethylene -2, 4,5-trichlorophenol -2, 4 ,6-trichlorophenol -vUlyl chloride endrin -lindane - -methoxychlor -toxaphene -2,4-D -2,4,5-TP (Silvex) D NC Department of Environment, Hu.Ith,&. Nawril Re.rnurces. SA?vIPLE Al'IALYSIS REQUEST St.ate l..J.boratory of Public Health P.O. Box 28047, 306 N. Wilmington St. Solid Wut.e Management Divi,ion Raleigh, Nonh Carolina 27611-8047 RiteNumber Nto 00 I loOIP a s-O lfarneofSite Cn·sfl' X Drum ,)J ft::, Sarnp!e!D Nurn CO·I03·SL 08/10/98 1310 GRAB 12345678 C0081098, NC 0. WILSON Collected By~ SOIL Siteloc:ition !1 X &.-cl IV C--DateCollected _ _,(;L ...... ..,...._,_~~~--1+--'~~~-- ORG·CLP Hazardous Waste Solid Waste _Duperfund Sample Type I) Environmental Concentr::1te Comments II Ground Water (I) Surface Water (2) -Solid (5) -Liquid (6) t-Soil (3) .'/ • '· ~ --Sludge (7) Other (4);: -Other (8) i---· ---,-----'----j Organic Chemistry Inorganic Chemistry - Acid:D/N Ext. 2,4-D_ ., 2'.4,5-TP.(Silvex) chlordane ~ Results (mg/I) -----··-- I= heptachlor hexachlorobenzene _____ _ hexachlorobutadiene -., ~----- 1 endrin '.J':. lindane (!. _ rnethoxyc_hlor toxaphene 1: 1-- I FOR LAB USE ONL y Date Received ?-//f-9?l(t, ()/6 .Date Extracted _________ _ Date Analyzed _C/~·-/~'f_-~q~lf°~-rl~d~- 1 Reported By 1 Date Reported Lab Number I DHS 3191 (Revised 12/93) 982667 Parameter Results(mg/l)(mg/kg) antimony arsen.ic barium beryllium cadmium chloride chromium cobalt copper fluoride iron lead manganese ______ _ mercury nickel nitrate selenium silvei- sulfates thallium vanadium. i.inc pH conductivity ______ _ TDS flash point ______ _ VOA Soil 10 TCLP Compounds Inorganic Compounds arseruc -barium -cadmium -chromium -lead - -mercury selenium -silver - Organic Compounds benze:1e carbon tetr.icWoride -chlordane Results(mg/1) Results(mg/1) ·-·· .-.---•-·· ------~-----·- chloroben::ene -chloroform -o-cresol -m--cresol - -p--cresol cresol - -1,4-dichlorobenzene 1,2-dichloroethane - -I, 1-dichloroethylene -2, 4-ri ich lo roethy I eoe -heptachlor bexachlorobenzene -hexachlorob uta.diene -~ hexachloroethane -__ methyl ethyl ketone nitrobenzene - -pent.achloropbenol -pyridine -tetrach.loroeth y le Ile -trichloroethy Jene -2, 4.5-trichlorophenol -2,4.6-trichlorophenol -vinyl chloride endrin - lindane - -methoxychlor -toxaphene -2,4-D --2,4,5-TP (Silvex) NC Department of Environment, Health, & Narural Rc.rnurccs SA~IPLE Ai~ALYSIS REQUEST SlAtc Laboratory of Public I-:Iealth P.O. Box 28047, 306 N. Wilmington SL Solid WuLC Management Divi,ion Raldi::h .. Nonh Carolina 27611·8047 lliteNumber /vtv Oo I ft; V lo 2 r:;:n Sample ID Numl, CD-103-SL 08/10/98 1310 GRAB _j_ . :i. , 12345678 C008l098, HC D. WILSON g"lameofSite Cr(sJl'Y ,Dcu tn .5;ib ,Colle<:tedBy_l SOIL . D If\ .J} ./ · ORG-CLP EXT /PCB Soll Site Loc:ition _,V"-_,,x'.~fz,_il'.,J.,_C,-1.(AJ.'J-'-. _...,/k--'-1_,l.-,::__ ___ Dale Collected 1 11 ~gency: Hazardous Waste Solid Waste ~fund TCLP Compounds ---- D Sample Type Inorganic Compowuis Results(mg/1) Environmental Concentr.ite Comments -arsenic barium - Ground Water (I) Solid (5) cadmium II -- -chromium Surface Water (2) Liquid (6) lead uZSoil(3) -- , -mercury Sludge (7) I . --se.e:imm ' silver - -Other (4): -Otber (8) - ~ - -Organic Chemistry Inorganic Chemistry - iParameter Results (mg/I) Parameter Resul ts(mg/ I) (mg/kg) Orgac.ic Compounds Results(mg/1) .. _ P~T:GC/MS -antimony benzene .. !./'Acid: BIN Ext. -arsenic carbon tetrachloride 11----2,4-D barium chlordane 2,4,5-TP(S'iivex) ----•--···--------··---. ·-· -· -. -· -·--..... -·---·---------··· ------·------·- -beryllium -chlornben.zene chlordane cadmium chloroform --- I beptachlor -chloride -o-cresol hexachloroben.zene -chromium m-cresol - -hexachlorobutadiene cobalt p-cresol ., -- 1= endrin copper cresol -- lindane •~r.-fluoride 1,4-dichlorobenzene methoxyc~ior --tron 1,2-dichloroethane --- 11~ toxaphene s. (i :J. SIi l -lead 1, 1-dichloroethylene -e_c. R 0, L'i.f¥{!j,. -manganese -2, 4-dichloroethylene -mercury -heptachlor nickel hexachlorobenzene --11-· . nitrate hexachlorobutadiene ---selenium ~ hexachloroethane . -- -silver methyl ethyl ketone -I FOR LAB USE ONL y sulfates nitrobenzene --- -thallium pentachlorophenol -Date Received ~-/tJ--'ff ({, W6 -vanadium pyridine -. ff\,(}, 8-1(). q JUI\ ' -zinc tetracbJoroethylene -I Date Extracted Pe.8.r '5?-:::l7-f_?l/P -pH -trichloroethy lene 7'C?Bf CJ-1-:[XP,. -conductivity -2, 4, 5-tri chlo rophenol TDS 2,4 ,6-trichlorophenol Date Analyzed 8i!/./:$-3/-1J --I Reported By -flash point -vinyl chloride. ' endrin --lindane -- 1 Date Reported --metho~ychlor 982668 --toxaphene Lab Number 2,4-D -- --2,4,5-TP (Silvcx) DHS 319 ! (Revised l :?./93) I • NC Department of Envi_ronment, He.11th, & Narural Resources .sAivIPLE Ai'IALYSIS REQUEST St.ale Laboratory of Public He.alth P.O. Box 28047, 306 N. Wilmington St. II Solid Wane Ma.nagemenl Divi,ion Ralcit:h, North C1.ro!ina 27611-8047 lliteNumber Nto 00 I loO& 51 s-D Sample ID Num If ameofSite Sitel.oCJ.tion Cn'.-,f,,x /Jrum. ,)J £ CollectedBy~ C0-112-SL 08/11/98 1720 GRAB 12345678 CD081098, NC D. WILSON SOIL () X /4,-c/ ( fl/ C--DateCollecte<I' ORG-CLP VOA Soil 145 llgency: I --Hazardous Waste Solid Waste _0uperfund TCLP Compounds -- D Sample Type Inorganic Compounds Results(mg/1) EnvironmenL'll Concentrate Comments arseruc -barium - Ir Grouod Water(!) Solid (5) -cadmium - -chromium Surface W~ter (2) Liquid (6) le:id --- -mercury m-Soil (3) ~;,: Sludge (7) se!eniurn --. ,. --silver ' -~-- -Other (4)'-i -Other (8) - ~ - ' - Organic Chemistry Inorganic Chemistry - f~r ·. Results (mg/I) Para.meter Results(mg/l)(mg/kg) Organic Compow1ds Results(mg/1) _ P&T:GC/MS -antimony -benzene Acid:B/N Ext. arsenic c:1Ibon tetrachloride I= -- 2,4-D barium chlordane ··•-·-••-·-·---· .. , .... ····-. .... .... ···-···-···-·-······---·· ----------2,4,5-TP(Silvex) beryllium cniorobenzene ---chlordane cadmium chloroform --'= hept.ichlor -chloride o-cresol --- hexachlorobenzene chromium m-cresol -- -hexachlon?butadiene cobalt p-cresol -- I endrin ~ ... copper cresol '"'-:; -- I ind.we } ,r.: -fluoride · I ,4-dichlorobenzene - -methoxychlor tron 1,2-dichloroethane --- 1: toxaphene lead 1, 1-dichloroethylene -- -manganese -2, 4-dichloroethylene mercury hept.ichlor --- nickel ·hexachlorobenzene -11~-- -nitrate hexachlorobutadiene - selenium ~ hexachloroethane -- -silver methyl ethyl ketone -I FOR LAB USE ONL y -sulfates nitrobenzene - -thallium pentachloropb~nol Dace Received 9-/L/ ~ ffley,){; - -vanadium pyridllle -zinc tetrachloroethylene I Date Extracted -- -pH trichloroethy lene - conductivity 2 ,4,5-crichlorophenol q -I ±-9 X-11,;1 --Date Analyzed TDS 2,4 ,6-trichlorophenol -·- .• Reported By -fla.sh point vinyl chloride - --endrin . lindane --I Date Reported --methoxychlor 982669 --toxaphene Lab Number 2,4-D -- --2,4,5-TP (Silvex) DHS 3191 (Revised l'.::/93) I 'ill· ,. ..:! ;~-,. 1· 1;·~ I NC Department of Environment, Health, & Narural Resources SMIPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wi!mint,1ton St. Solid Wuu: Muugcmcnt Divi,ion Raleigh_, North C1.roli.na 27611-8047 I Site Number ft!Cv Oo / (p V lo:? s=n SampleIDNuml C0-112-SL 08/11/98 1710 GRAB ~ · , 12345678 CD081098, NC D. WILSON ,n . _j_ l)' .. < :j_ . SOIL m·NameofSite «r(Sfl'Y ;_Cu tn 01(, ,CollectedBy--c ORG-CLP EXT/PCB Soil SiteLocation~V~'/~/{~,-,...,~,,_~_,__//J~~L---~_· __ DateCollected ____ -=======--=1=4=6=====- 0 Agency: __ Hazardous Waste __ Solid Waste ~fund D Sample Type Environmental Ground Water(!) n :;::rface \Yater (2) n-Soil (3) r _ Other (4), , Concentrate -Solid (5) -Liquid (6) -Sludge (7) -Other (8) I Organic Chemistry I Parameter Results (mg/I) ~T:GC/MS • _ ,d:B/N Ex:. I . ---2,➔-D ,< ·-·-----··-·-··---·--. -2,4,5-TP(Silvex) chlordane - -he?tachlor I hexachlorobe:uene - -hexachl6rpbutadicne I -e:::drin -!Ulciane/~ . -methoxy~hlor toxaohene I -~ r}_t:, & :, < 0, t_O /fY'1 I ~ - -I - FOR LAB USE ONLY I Date Received f;j_tf=f'j'vP,'r,11/6 e .za~ qe-;,.,., I Date Extracted{!_f!J,; ?~ '1-9?'VP ?CBi-9_-/-9!i'Yp_ Date AnaJyzedAN/J:l-3/ -'J£iit!J I Reported By 1 Date Reported Lab Number 982670 I DHS 319! (Revised l'.2/93) Comments Inorganic Chemistry Parameter Results (mg/l)(mg/ kg) antimony arsenic • barium -----boryllium cadmium -chloride chromium -cobalt -copper fluoride -iron -lead - -manganese -mercury nickel -nitrate - selenium -silver -sulfates -thallium -vanadium -zinc - -pH -conductivity TDS -. -flash point TCLP Compounds lnorJanic Compounds arsenic -· barium cadmium chromium lead mercury selenium silver Organic CompowHls ben2ene carbon tetrachloride -chlordane Results(mg/1) Results(mg/1) --., ·--·--·--·-··-----·----·-·. chlorobenzene -chloroform -o-cresol -m-cresol - -p-cresol cresol - -1,4-dichlorobenzene 1,2--dichloroethane - -I, 1-dichloroethy Jene -2, 4-dichloroethylene -beptachlor hexachlorobenzene -hexachlorobutadiene -~ hexachloroethane -_ methyl ethyl ketone nitrobenzene - -pentachlorophenol -pyridine -tetrachloroethylene -trichloroethy lr:ne -2,4,5-trichlorophenol -2,4,6-trichlorophcnol -vinyl chloride endrin -lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Silvex) I NC Department of Environment, Hc.alt.h, & Nawral R~ourccs SAMPLE Al'IALYSIS REQUEST Sta.te Laboratory of Public Health P.O. Box 18047, 306 N. Wilmington St. Ra!ei1:h, North C.arohna 27611-8047 I Solid Wute Man.agcmcnt Divi,ion iteNumber Alto 00 I loo& a s-O ltameofSite Cn·.sfl'x JJ/um ,sle, Sample ID Numl C0-126-50 08/10/98 1650 GRAB 1 12345678 C0081098, NC O. WILSON SiteLoe-1.tion cQ_ f fo,-1',/ f1J L---, ( lgency: I --Ha=dous Waste Solid Waste Duperfund TCLP Compounds -- Collected By_ I ORG-CLP Date Collected • VOA Sediment 94 D Sample Type Inorganic Compounds Results(mg/l) Environmental Concentr.ite Comments arsenic -barium -u-Ground :,Yater (I) Solid (5) cadmium -- -chromium Surface W,ater (2) Liquid (6) !e:id --- : -mercury II-Soil (3) .. \. --Sludge (7) -selenium \·-.. silver . ,", --Other (4).1\,:· -Other (8) - i •. - -Organic Chemistry Inorganic Chemistry - ·(P~r Results (mg/!) Parameter Results(mg/l) (mg/kg) Organic Compounds Results(mg/l) · _ P&T:GC/MS -antimony -benzene 1: Acid: BIN Ext. arseruc carbon tetrachloride -- 2,4-D ··-·-·-·-·-·-·-· --·-« -•· ·-··. -·--·· barium chlordane 2,4,5-TP(Silvcx) --· ·-·-----------· ------------ beryllium chlorobenzene --- chlordan_c , cadmium· chloroform I ---heptachlor chloride o-cresol -- hexachloroben.z.ene --cluoc.llum -m-cresol -hexachlorgputadiene cobalt p-cresol -- I endrin , :,., copper cresol t• --lindane :.,-: fluoride 1,4-dichlorobenz.ene . , -- -methoxychlor -iron 1,2-dichloroethane - I= toxaphene lead I, 1-dichloroethylene ' -- -manganese -2 ,4-dichloroetbylene mercury heptachlor ---nickel bexachlorobenzene -11= - -nitrate bexachlorobutadiene -,<ielenium ' bexachloroetbane -- -silver r,;iethyl ethyl ketone -I FOR LAB USE ONLY -sulfates ni1robenzene - . ;?'-/(t-wew6 -thallium pentachlorophenol -Date Received vanadit.:m . pyridine --zinc tetrachloroethylene I Date Extracted· -- -pH trichloroethylene - 1-/J/ -q~ 111 -conductivity -2, 4,5-trichlorophenol Date Analvzed TDS 2, 4, 6-t richlo rophenol I Reported ~y -- -fl:~h pcint vinyl chloride - --endrin lindane --I Date Reported . --methoxychlor 982671 --toxaphene Lib Number 2,4-D -- -2,4,5-TP (Silvex) DHS 3191 (Revised 12/93) -I I NC Dcpanmcnt of Environment, Hu.Ith, & Nawral Rc.&ourcc, SMIPLE Ai'IALYSIS REQUEST State Laboratory of Public Hc.alth P.O. Box: 28047, 306 N. Wilmington St. fl Solid Wute Marugcmcnt Divi,ion Raleii:h_, North C.aro!ina 27611-8047 OSiteNumber rev Oo / fe V lo :;; s:::n Sample ID Numb, C0-126-SO 08/10/98 1650 GRAB 12345678 C0081098, NC 0. WILSON lt ameofSite Cr(sff'y J)d; W1 ,:if ,Collected By·_ ,.,_, {£. ORG·CLP EXT/PCB Sediment SiteLoc:ition {) 1[:fvJ,-~ /IJ l--DateCollected_· ___ ----;:::===::::'::..... __ -_;·:.___9_5 ___ _ DAgency: __ Hazardous Waste __ Solid Waste· ~fund TCLP Compounds II Sample Type I) Environmental Concentrate Comments Inorganic Compounds -arsenic Results(mg/1) barium -m-Ground Water (I) -Solid (5) Surface .\Yater (2) Liquid (6) -- -cadmium -chromium -le:id I-Soil (3) .;j -Sludge (7) J/'other (4r1 -Other (8) I l . · -men:;ury selenium - -·silver - Organic Chemistry Inorganic Chemistry -.~.--I r Parameter '. rl . _ P§:T,GCIMS 11 '. 1 ,._if 1 _i/2cid: BIN Ext. Results (mg/I) Parameter Results(mgll)(mg/kg) Organic Compow1ds Results(mg/1) j ____ 2,4-D I _ 2,4,5-TP(Silvex) chlordane heptacWor 1= hexachlorobenzene _____ _ hexae:h1or.9butadiene ------I _ endrin lindane -,;; -methoxv~hlor -.. , I _ toxaphene · l...k'."' PCB -; 1= <O•[Of,OM , I FOR LAB USE ONL y Date Received ~f/--~e6' I Date Extracted ~ztjj 'A:B} q-1-~ . Date Analyzed h,J,4g-3/·9'f'~ I Reported By I Date Reported _________ _ Lab Number •~~~_6J"':Z , I DHS 319 l (Revised 12/93) -antimony arsenic -barium ·--- -beryllium cadmium -chloride -chromium -cobalt - -copper fluoride -iron - lead - -manganese -mercury nickel -nitrate -selenium -silver -sulfates -thallium -vanadium - ZillC - -pH -conductivity TDS - -flash point - - - - - - benzene carbon tetrachloride -chlordane ---··-···---·--·--········· --. --· chlorobenzene -chloroform - o-cresol -m-cresol - -p-cresol cresol - -I, 4-dichJoroben.z.ene -1,2-dichJoroethane -1, 1-dichJoroethylene -2, 4-d i chi o roe thy I ene -beptachlor hexachlorobenzene -hexachlorobutadiene -~ hexachloroetbane -_ methyl ethyl ketone nitrobenzene - -pentachlorophenol -pyridine -tetrachloroeth y Jene -trichloroethy lene -2,4,5-trichlorophenol -2,4, 6-trichlorophenol -vinyl chloride endrin -lindane - -methoxychlor -toxaphene 2,4-D - -2,4,5-TP (Silvex) . ') I g 0 m I I I I :I I I I I I I I I I I NCDEI-INR Divisi of \VastC Man_agemcnt uperfund Section D Hazardous Waste Section D Solid Waste Section Organics Lab: L-- Inorganics Lab: __ CHAIN OF CUSTODY RECORD ProjectName: lcts±tx Dn11b 51·f,<_. Site ID# (NCD#) Do I & O (ft a 5:"D - Location :__j)Q,L......J,.y,......if-ae--CLJc~c"'-J__,_, _.(\)=-'=(____=--- Address :_.,,1,T--=1-0-'-"d"'-u""-l.s....1±!.!....r-"'8~---"I-Dµ;__r~, __ Sampled By: Donn a. W i' Is o n Sampler ID __________ _ Telephone:~ '73 3 -2 go I X J-rJ Date Sampled: g;IJ/ 'It"-ff//'-//? f:' r ~ I Time Sampled: Sample Types: Soil /~ \.Vater ~Waste ---Other --- F, <Id 5 ~"'fl• t>'> ~ft~~ CD-0o1 ~,s L (,) • co -oo 1 -s L('.~) · e o -ooz -r.,,0(2.z.) , co eoz tr w(z4 'i · CD--002.-s-t.(i) ) ) . . ) /) . ! Co -Ot>2--S L ( ,); C. D -003 -S ~(7) j co -oo "3 -st-.{,); c.D -ov ':I -5 L (n)) CD 00 '1-5 L{L9J' {;D_:t,o~~zl ,~) <!to ---oo.5""-~ L {n)) tO -oolQ crw(u.)) CO-oo~ -<,-u.> {2~)) Co o"D/o 5L {tq)j Co-001p SL(~; Ca--00:1-.n{ ~ t O -Do1 ->L /21"\• CD ~oO'iJ--j I. I 33, · Cr. --009.-S J... I " CO -oo<l-5L / n \ · c l!J.nlrz.,.y"lf·,~ > \ , , Field Sample co-o;z.-;~/;'-13), CD-O/.l-&-'• Y3,,"')o C D-oa/q,') • CD-Dl'-f.-.5D('I~) '. co -01'( -.5D(l/1)' CIJ--01,-rn{ ,1 Is'/) rf,-"'l' // l~ ;J ✓1 t->J !I Numbers co:.o,s-,o-(s-2); C,O~{)/j;-50c·s:0 . co -o I (a 5 D(s:,\. C.D-D17-5L(<w)' co-~~\ ... . ,,, / -/ ) /J j ~ l!..0 -oJ,g ~L(il~C. 0 -o I S-5 L(i17) J C.D -o 1q-GW (11q) J Co -o 1q -(-,-w (1-z'); Co-011-:,Ll1z.3)~ CD-01q--SLl1z.'-1\~ c.o-01CJ-swf,2.(,"\~ ctJ-01q-5w(1zs\ RelinquishedBy: --:S-111,cc'--1,711J--!.,,, Date: c;:?~rf.j'p Time: /2--'SO _______ i_,;rS!.'1iow.nillat·"-'-ur8e'c..--={'~/_~ _______________________ j Received By:._---"'-0'--=~-----="-<---=----=·.,d=--:,...,,.£<-=~::......c.· -'-=bZ._.---"='---Date: g:-/¥ -97 Time: p :50 .. , (Signature) Relinquished By: _____________ _ Date: ----Time: ----ISinnature' Received By: _______________ _ Date: ----Time: ----(Signature) Relinquished By: _____________ _ Date: . ___ _ Time: ----fSionature~ Received By:. _______________ _ Date: ----Time: ----(Sig~) Results Report;~ ~ ~ ~ I ,; ~_ifC) --, . •. . ·~~DEHNR ' ' Divisio of \Vastc Management I perfund·Section · D' Hazardous Waste Section . D Solid Waste Section g CHAIN OF CUSTODY RECORD Organics Lab: ~ Inorganics Lab: __ o============s=================;i Project Name: Crrs +ex "Do::t.1 · Sampled By: Pon n Ci IAJ; IS o 11 E Site ID# ( ' · Sampler ID _________ _ Location: Telephone:~1.3:s-Z$DL 'l::,3)7 II Address:_~u.LL<L.2-1..LJ4--'I-L-'--~-Date Sampled: ff/10/19: -Z/!Y/9~ II lk===================1,,,;T~i::m:,:e~S~a:m~p::,;l~e,:d;;;;: ;;;:;:;;;;;;:;:;;;;;;:;:;;;;;;:;:;;;;;;:;:;;;;;;:;:;;;;;;;';;;:;:;;;;;;:;:;;;~~j Soil~ Water ;,-----waste __ _ I Sample Types: Other --- ~ . . . . ' --rW (JO •-~ C YJ -o -& L,V (p2. • CD --4 ' C -l(fD5); 'co -o - - C!.o -o I Si 0 nature I Receive'd By:_-1<'~~-==-· ~.J=-c·~0;~~'-'--'. ='-"---- (Signature) I Relinquished By: Si nature I Received By: (Signature) I Relinquished By: Si 0 nature Received By: I (Signature) Results Reporte I I Date: 'F, 14--78 Time: Date: [[-/'l-9'6 Time: /.:<:St) Date: Time: -------- Date: Time: -------- Date: Ti1ne: -------- Date: ___ _ Time: ---- 1•·:··· .. NCDEHNR IIJ?ivisi,suJ-of \Vastc Management Organics Lab: 1--- Inorganics Lab:_-__ ll~perfund·Section · . □· Hazardous Waste Se"ction · 0: Solid Waste Section I m . CHAIN OF CUSTODY RECORD Project Name: C..r:t::i+e~.'D Qi.A vn. ~ i+ e.. Sampled By: VJ ;n..; --.,,. L0 ; I <; °"' Sit, ID II (NCD/1)~1;1, ~ Sampler ID Telephone:Ci!!i) ,3 3-Z-~Di f... 3J.,7 Location:~~ tJ L-g Address: ,() , Date Sampled: '8j!o/1<i-/ 7 9! . Time Sampled: , u Sample Types: Soil ~ Water ~-Waste Other . 0 ~: ;;1~ ~~~\ ,.,Gld 0-':/ ~ CO O'iQ Sw{/'to)jCD IDZ·f,u){fl6);G9 r'.,O~03-SL {tv) •) CO -103-S L ( 11); CD-IIZ.-iL?i~Q; Co_-112:..~i,f_l'i.<i) CO -113-r.u.J /43)• CD -1-z.t-so /q'I\•. co-;2.1,;,-:Sof<rs-\· , , 0 D D n D 0 0 0 0 0 E Field Sample C.o.=1.~_'2-J_w(_q_~_o -12ia -$ LU (qq)_;__co -1 oo ,...T!3 (l'f '6) J-_ . Numbers to -21?0-R B ( 1s:z..); co -z.oo:...RB (15"'1)· Co -'to0-128 (L~· Cn-4vo-v51' . _) -; .. , Relinquished B/ 751, 111 _ C.. \ [0A~-Date: 't:S"lq -98 Time: (Z CS<.:i fSionature\ {,/ Received By: '--t/'~ J.t?~ Date: T-1~ -'10 Time: /.::?:So (Signature) Relinquished By: Date: Time: rsi 0 naturc' Received By: Date: Time: (Signature) Relinquished By: Date: Ti111e: foi 0 nature\ Received By: Date: Ti111e: (Signature) . . . ;t T ./ /4"' './t _/ Date: .~::ZL:_f.f'"Tin1e: Results Reporte . -11, -~-. · · (~ture) . . ~, s9) STATE LABORATORY OF PUBLIC HEALTH I I P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS ..... ...., ,., "~n .... ~ , 'I/~, "'Cl. ~ BASE/NEUTRAL ANO ACID LAB NO -, , ./ I EXTRACTABLES FIELD# {!j)-/JO 1-S '--/17\.-c,O:J-C:I ~75-oo3-SL "71-vo<I-SL COIIPOUNO TYPE ( .3 l ( ;;/ ) ( 31 ( ~ l UNITS _ _..✓..;;/ka ..,......_. .. n/ka _,,,.,,,,n/kq ,ra:1:,1( .. n/kal N-nitrosodirrethvlamine IOI Cl'<O i .I -' -~ ' (2 chloroethvllether h 1 ormheno 1 phenol ·13-dichlorobenzene 4-dichlorobenzene .2-dichlorobenzene is(2-chloroi s=r=vl lether xach 1 oroethane , nitroso-di-n_nrrv'lvlamine nitrobenzene ~horone trnnhenol 2 4-dirrethvlohenol · ts (2-ch loroethoxvlrrethane 4-dichlo~henol .2.4-trichlorobenzene anhthalene xachlorobutadiene 1 crh 1 oro-m-creso 1 lxachlorocvcl~ntadiene 4.6-trichlormhenol -ch loronaohtha 1 ene acenaohthvlene ··rrethvl ohthalate 6-dinitrotoluene acenaohthene ' ?,4-dinitr=henol sa, ·,r,,50 U 4-di ni troto 1 uene 10, .'l'.=iO -n i t r=heno 1 ,o, ,,,_i:o fluorene /0 '~30 nchlor=henvlohenvlether ethvl ohthalate J, 4 6-dinitro-o-cresol so, ~f,,t;f) ('i ohenvl amine /0/330 l>"obenzene '-brnmnhenvlohenvlether hexachlorobenzene ~ ft:ntachloroohenol so/N,So ienanthrene //1/ ~~o anthracene .-i,butvl ohthalate / / , ■fl uoranthene " ' ' \ m'DL ' -Estimated value. f(.,_o/.SO/ J... -Actual value is known to be less than value given. '"7 Y..HA.-::{ 1' ".0-<1".--.SL- ( 31 _,_,,, .. n/ka · ' - , ' ',(;. 0~ i,L -Actual value is known to be greater than value given. U -tlaterial was analyzed for but not detected. The nurber I -Not analyzed. is the .!1ininun _Qetection !:_imit. m"])L --Tentative identification. _ -On NROC List of Priority Pollutants. I , ~~ , n })-~-SL ( :al ) ,,m,J/" •0 /ka\ . , , ' I I I I g D 0 I I I I I I I I I I BASE/NEUTRAL ANO ACID EXTRACT ABLES COMPOONO nvrene benzidine butvl benzvl ohthalate benz(a)anthracene chrvsene 3 3-dichlorobenzidine bis(2-ethvlhexvllohthalate di-n-octvl nhthalate benzo(b)fluoranthene benzo(k)fluoranthene benzo(a)nvrene i ndenc ( 1 2 3--cdl nvrene dibenzo(a.h)anthracene benzo(a h. il=rvlene aniline benzoic acid benzvl alcohol 4--ch I oroan i 1 i ne di benzofuran 2-rrethylnaphthdlene 2-rrethvl aheno 1 4-rrethvl oheno 1 2 nitroani line 3-nltroani 1 ine 4-nitroaniline 2.4 5 trichloroohencl J-1 T I Jl 0/'.,n:: Roµ<., J -Estimated value. STJ,TE LABOAATORY Of f'\JBL!C HEALTH P.O. BOX 28047 -306 N. ~ILHINGTON, ST., RALE[GH, N.C. 27611 ORGANIC CHEH[CAL ANALYS[S LAB NO ·~ -'IJ..,""' 'l':l,"11'"'</ 'IP;J(,:Jln ,no'}/ c::J )t' FIELD # P71-ool-.5L ,, z,-002-:SL ~-l\-o<:B'-SL eJJ-oo'/-.,;;.i.. TYPE ( :; \ (~\ ( ~ ) (31 UNITS ,.....;,;/ ""/kn .,...-,✓.:;,/kn .. .-v l,n/kn -ua/ka /0/~30 I • IA. ' -l r'n /,1.<o / /01.330 " i3oi,- . .I, ~ ::l,,-.,1<'.: so/11.so IA 107330 IO/.s.:.o .so/J1,,,11 I , I / \ , \ ' ' \ ..-oh1.ro " . IA--I.A..-vL .. f 101.=o ~· ... S'o/,u::o . , I ', • I '17 ,1 \ -,.........__ +I-r-J 7 -..., 7-+) c+j . -- frlJ)I- HzO/ Soll.. to be less than value given. _,, 30 (Z) ..CCS"-.SL (-3' .....ul'., n / k a IA- / ' ;,,,:2.r1v IA-- I . IA--- , ' , ~ ( -r J - K -Actual value is known L -Actual value is known U -Haterial was analyzed NA -Not analyzed. to be greater than value given. for but net detected. The nuroer is the Hinirrun Detection Limit. 1/ -Tentative identification. fl -On NROC List of Priori ly Pollutants. o/',t' ..1/...:;>,2 Ci>-~::5L ( 2\ _,,_-r ·"/kn> v<- I . I I ,l - , - ( -} STATE LABORATORY Of PUBLIC HEALTH I I P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS BASE/NEUTRAL ANO ACID LAB NO 1r,1CJ '1/ "JH. <-fY ·-,, ::,,1_ 'A ~1/~ V •1V2/A£10 EXTRACT ABLES FIELD# IIT,) -Od7-:5,L-('i'l-<XJf<-S/... ~l)-QIJ<I-Sl, n_J)-<)n-<I COMPOUND TYPE ( ?, l ( ;:i l (3) ( ~l ._il',,n/ka ~ .. n/ka -...L.l,.,,../kn . .••••.✓.:a/kn UNITS -nitrosodimethvlamine If\/ <!:10 I• ' , -i ,t . " - s(2 chloroethvl)ether c chlornnhenol henol 13-dichlorobenzene 4-dichlorobenzene 1.2-dichlorobenzene Is (2-ch loroi snnrnnv\ )ether xach 1 oroethane N-nitroso-di n-nrnnvlamine · trobenzene horone c nitroohenol 2.4-dimethvlohenol us(2-chloroethoxvlmethane 4-dichloroohenol l 2 4-trichlorobenzene ft;htha l ene .xachlorobutadiene 4-chloro-m-cresol .xachlorocvcl~ntadiene 4.6-trichloroohenol c chloronaohthalene acenaphthvlene (methvl ohtha late 6-dinitrotoluene acenaohthene 4-dinitrnnhenol sa, 'foSO 4-dinitrotoluene /()/ ~:io 4 nitrnnhenol .-ro1 ,_-:o f:"orene /OI '30 chlornnhenvlohenvlether ulethvl ohthalate " 4 6-dinitro-o-cresol 50, i1-,o ·ohenvlamine /0/330 obenzene 4-br~henvlohenvlether ltachlorobenzene " ntachlornnhenol sol11n:ro ohenanthrene J/l/_:r::i0 lthracene butvl ohthalate I I I , . 1 uoranthene \ , \ I ' \ rn1) L I -Estimated value. H,.o/S0/1 .... -Actual value is known to be less than value given. q V ,/4 </:.1 n--,..-01<1-.">l'l ( ,L, """' ',,n/kn . . I .. ,_ '7 I A - . ·• , ' A ,o.i-· IIL. , •I L -Actual value is known to be greater than value given. -Not analyzed. t. -Material was analyzed for but not detected. The nurber is the MinirTUTI Detection Limit. m'])L -----Tentative identification. ~/ -On NROC List of Priority Pollutants. I c;.v "J/ ,! .,,, n7\ .• 11J.<-. <;;) ( L/ l , "··""/kn ~, ., , I ro/)n , ,. , .., /ft, ft "7 u / ' I I I I I I I H D u D I I I I BASE/NEUTRAL ANO ACID EXTRACT ABLES COl1POONO nvrene benzidine butyl benzvl ohthalate benz (a) a.nthracene chrvsene 3 3--dichlorobenzidine bis(2....,thvlhexyl)ohthalate di-n--octvl ohthalate benzo/blfluoranthene benzo(k)fluoranthene benzo(a)nvrene i ndeno( l. 2 3-cdl nvrene dibenzo(a h)anthracene benzo(a.h i ln,,rylene aniline benzoic acid benzvl alcohol 4-ch 1 oroan i 1 i ne dibenzofuran 2--methvln>nhthalene 2--methvlohenol 4--<rethvlohenol 2-nitroaniline 3 nitroanillne 4-nitroani line 2.4 5-trichloroohenol H I I )t<.O(' DP '"-DA.Jc., STATE LABOOA10RY OF PUBLIC HEALTH P.O. BOX 28047 -306 N. ~ILMINGTON, ST., RALElGH, N.C. 27611 ORGANIC D1EMICAL ANALYSlS LAB NO 9'1' -,, -.;/ <.t q f :v--<{,,, 1 'f O..:,L, -<V </.JIJ/,% FIELD# f'7\ -007 --c i... C.7"> _,.,o',l · SL />?J-.:>o9-:SL ''"-ot.J...<:i... TYPE ( 3, ( ~) ( 3) ( ·-s l UNITS .. ..-L1I .,., I kn .. ~ /kn ~•·ua/kn __. ,t .. n/ka /0/?30 I,(__... 1 ' ' ' ,A . 1..-,, 1,,.,.0 /0/330 . . ~t. ,;o SO/ 1()1330 IO/.s3o SOh"2'iO / / I r ,/ • F ~ ' I <oln.~o IA..-IA-l -l . .. ✓ 1ol."C£0 ,J,- s-ol,t.~o I I / / ,J, \ \ \. -~ ~ ~ -1-1-I -J /-) { -J r-J . - m:D1- J -Estimated value. H2.0/ SOIL K -Actual value is known to be less than value given. ~"~'"'~'fr,)_ C'"·ol<I·~-,., r LJ.1 ....... ,,n/ka " / .... , I ,4 - , \. ~-n/C vL. / ' -I' ..J-) - L -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. The nunt>er is the Minim..rn Detection Limit. ~ NA -Not analyzed. 1/ -Tentative identification. ~I -On NROC List of Priority Pollutants. '.,.,, I ., ~ ""-0/S· .sl> rl/ l , /ka'\ I, , \ I I / ' J l'ln n ., J / I \ I -r+J - I STATE LABORATORY OF PUBLIC HEALTH -' .. ' PO BOX 28047 306 N WILMINGTON ST RALEIGH NC 27611 ORGANIC CHEMICAL ANALYSIS BASE/NEUTRAL ANO ACID LAB NO 10(1 ::J/_, l/_ (IC,:JI.CJ V d 01. 5D 'fJl.,)1-..,_, ury_7/.,::;;(/ <.J p ~~ I - EXTRACTABLES FIELD# ;,1)--0/t .:--<:;j) ('fi-r,/7-<L "J)-O/ "'-SL (!.?)-019-S L 1>1)-02/ -SL 1"7>-o::> :2-5L COl1POUNO TYPE ( LJ ) ( ~' ( . ') ( 31 ( ~' ( 3, UNITS ....,,,.,,,. n /kn ~ •"/ko __ , ··/ko ' /ko ~ .. ,/ka -~"n/kn'\ N nitrosodirnethvlamine Ir.I .;j''!O -, , ', . -IA IA ~ IA -i, - s(2-chloroethvllether ch l or...,heno l □henol 13-dichlorobenzene I 4-dichlorobenzene 1.2-dichlorobenzene ~-O"" t' (2-ch l oroi """r""v] l ether A xachloroethane -n i troso-di -n-I'lrl'V'lvl amine nitrobenzene 1nnhorone nitroohenol 2.4-dirnethvlohenol s(2-ehloroethoxv)rnethane 4-dichlornnhenol l 2.4-trichlorobenzene hthalene xachlorobutadiene ~;...chloro---m-cresol hexachlorocvcl~ntadiene 114 6-trichlornnhenol ILchloronaohthalene acenaohthvlene ftirethvl ohthalate 6-dinitrotoluene acenaohthene '4-dinitr...,henol SOI 't,,So I 4-dinitrotoluene I 101 .'?.~O I nitr=henol .,01 ,. "'O fl uorene /0/ 30 -chlor""henvlohenvlether iethvl ohthalate " 4 6-dinitro-o-cresol SOI ,,._,:-0 I iohenvlamine /01330 7obenzene -br~henvl □henvlether ~xachlorobenzene ~ ?ntachlornnhenol so/11,,:ro 1enanthrene //1 I ?'JO anthracene ibutvl ohthalate I I I , , , luoranthene \ , " 'I ,, I . ·--· ' '\ I rn1) L ~ -Estimated value. l-{,_o/S0/1- -Actual value is known to be less than value given . . -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. The nurber t -Not analyzed. -Tentative identification. _ -On NROC List of Priority Pollutants. is the _!1ininun _!!election ];_imit. mIJL - I I I I I I I I g D D D D D E m I I BASE/NEUTRAL AND ACID EXTRACT ABLES COMPO.IND nvrene benzidine butyl benzvl phthalate benz(a)anthracene chrvsene 3 3-dichlorobenzidine bis(Z-ethvlhexyllohthalate di-n-octvl ohthalate benzofblfluoranthene benzo(k)fluoranthene benzo(a1nvrene i ndeno( l. 2. 3-cd)nvrene dibenzo(a h)anthracene benzo(o.h ilnPrylene aniline benzoic acid benzvl alcohol 4-ch l oroan i l i ne dibenzofuran 2..,rethvlnaohthalene 2..,rethv l phenol 4-methvlohenol 2 nitroaniline 3 nitroaniline 4--nitroaniline 2,4,5-trichloroohenol H 'IJJ1t.1" ,, ✓J ..... 1£ ., J -Estimated value. STATE LABORATORY Of PUBLIC HEALTH P.O. BOX 28047 -306 N. WILMINGTON, ST., RALElGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS LAB NO ·x, ,, , 1 GJ Sl,7/~lJ y 'I J1,;"'/~-.o qJl,)I, ~:;2 FIELD # t""lJ-,;; (,-<,'/ ni)-017-<:1_ (!1)-01-;>-(l, /17'-olf-O TYPE ( £/-l f ~I ( -) ( . :1 UNITS -nn:7-u ,,, /kn un/ko /kn /kn /o/~:io • .... I , ' ~,, /,1,,,<o . I 10/_:130 'J/ ~.:v-, v . • A - "IL.SO SO/ I0/330 /O/.J3o so/!Mo I I I / ' ✓ -" ' I ' 1<oli1,,~o \A.., I ·~ IA . ~ '· I 10/=ri • .-S --~ l /\.-,, s-0/,1..,:;o I I / / ~, ' \ I "\ ' I ---.,..--._ --' ..J-1-( . ..J.. J l -I-J ( -1 1-J '---' ----- m1H- H.:.OI Soli.. to be less than value given. .'1.lrl, ',,_",I/ ,r71 -/1 /-:SL ( . l -~ .:c./ko j r .... I l .A. . I ' ~ {-} K -Actual value is known L -Actual value is known U -Katerial was analyzed NA -Not analyzed. to be greater than value given. for but not detected. The nurt,er 1s the Minirrun Detection Limit. 1/ -Tentative identification. ~I -On NRDC List of Priority Pollutants. • OP"lt,,",/~ <!.2J•o22:5L ( ~, ,.,,;.,/ ••"/kn "'I I~ / \ I , / ' -1-l - I STATE LABORATORY OF PUBLIC HEALTH (j) PO BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS BASE/NEUTRAL AND ACID LAB NO ,_,, v "I/ -,C ',/ !}Ol"J/ , '1 r~ o·,/ / , "IIJM"'', 'I V''j/ I ~• G1 ~., 1/ /,V EXTRACT ABLES FIELD# (']J-0.7-3-5L. /171-07-/-<.7> "'.])-OZ'S"-<:. 7 ,,.,. .AZb-S.J) ~~-0.:.3-<,·1 /7-,.,_ ,;,2_ a I COl1POOND TYPE ( ~ l (iJ \ ( J. \ ( '/l (..31 ( ~, UNITS ,..,;,.ii; , n/ kn --<.U"., "I kn ~,a/kq , .....,,..,.. "e I k a .....m;, " .. e/ko """'2(., ~ /k a) N-nitrosodimethvlamine I" I :,"(J 1..--•• .. -,, . -" s(2-chloroethvllether chlornnhenol ohenol . 'l3-dichlorobenzene •/ / 4-dichlorobenzene -{, or: ' / 2-dichlorobenzene ?J 3,-, le. .3 3<)J.• f,s(2-ch loroi <00rnnvl l ether I Ac -IA- xachloroethane nitroso-dl-n .nrl'V't."lamine nitrobenzene bhorone trnnhenol 2 4-dimethvlohenol I ts(2-ehloroethoxvlmethane 4-dichlo~henol 2.4-trichlorobenzene ~hthalene achlorobutadiene h l oro--m-creso l hexachlorocvclOOPntadiene I■ 4 6-trichlornnhenol l(chloronaohthalene acenaohthvlene methvl ohthalate 6-dinitrotoluene acenaohthene 4-dinitrnnhenol SOI 'hSO I 4 dinitrotoluene 10, '.'l'.'10 ~nitroohenol ~01,,.co fluorene /0/~30 lltchlornnhenvlohenvlether ethvl ohthalate J, 4,6-dinitro-o-cresol 501 \u:·o I iohenvlamine /0/330 17obenzene -brn>nnhenvlohenvlether exachlorobenzene ~ / entachlornnhenol S0/N,5'0 ,enanthrene //1 /::r::io "'f-jQV anthracene I A.- ebutvl ohthalate I . . , uoranthene ~-' / \ • I ,I/ • I ,/ m1)L ~ -Estimated value. 1-{,.o/SO/L- -Actual value is known to be less than value given . . -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. The nurber It -Not analyzed. -Tentative identification. -On NROC List of Priority Pollutants. is the _!!ininun_Qetection !;_imit. m])L - I I I I g u u D D E I I I I I BASE/NEUTRAL ANO ACID EXTRACTABLES aJMPOONO n"rene benzidine butyl benzvl phthalate benz(a) anthracene chrvsene 3.3-<lichlorobenzidine bis (2-€thvl hex vi l ohtha late di-n-octvl ohthalate benzo(blfluoranthene benzo(k)fluoranthene benzo(a)nvrene i ndeno ( l , 2 3-cdl nvrene dibenzo(a.h)anthracene benzo(o h i lnerylene aniline benzoic acid benzvl alcohol 4-ch l oroan i line dibenzofuran 2-<rethvlnaohthalene 2-<nefhvl oheno T 4-<rethvlohenol 2-nitroani line 3-ni troani 1 ine 4-nitroaniline 2 4 5 trichloroohenol J-l'f,1)£01'~ '·"'·• !5 J -Estimated value. K -Actual value is known L -Actual value is known U -Material was analyzed NA -Not analyzed. STATE LABORATOOY Of PUBLIC HEALTH P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 OOGAN!C CHEMICAL ANALYSIS LAB NO <.N ;ie,-c 'Ji' , <:>o (./f) J ,_,, "I' X 1/,b '-I Ito 9:U,l~IA FIELD# A2),oJ.:f-<i.l A:J> .,-i V. 51) f''h-15')',-'7 /'1\-,,X. -51) (':JJ-033-5<... TYPE ( ~ l ( I.fl ( LJ.) ( I I\ ( ~) UNITS nm!,11"; , n I k o ,....,,,,,, un/ko -.. /,n/kn /ko ~ .. n/ka /0/'"'0 IA..-I # , -., I A -I A l~n/,,.So 101 :130 . it.So SOI 10/330 1/0/.s.◄O so/tMo , , ✓ , I ,/ ' ~ I I "I ' I <o 1,,,,,.0 j .A -u -I , 1 A l ..I - ... ✓ /0 /_=r-111 "' s-ol,t..,o I J / I , ,, ' I ' ' ' • I -----.,............_ -j-/ { -J /-} r - ' ( -J 7~} --~ m1H .. HzOI Soll.. to be less than value given. to be greater than value given. for but not detected. The nuroer is the Minirrun Detection Limit. fl'J:ZH .. -1/ -Tentative identification. ~I -On NHOC List of Priority Pollulants. .av•,1J._v ('7) -/()3 5L. ( _,, ...• .d -/kn ) IA- 7 ' ., I . ~ -7 , . , ' ., - I ' ,, +l STATE LABORATORY Of PUBLIC HEALTH -' . ' ' PO BOX 28047 306 N ~ILMINGTON ST RALEIGH NC 27611 ORGANIC CHEMICAL ANALYSIS BASE/NEUTRAL ANO ACID LAB NO u· '_• I ') -,~ 7-1 EXTRACTABLES FIELD# 1171_,, 1_<:J -V171. i UA < ,,, COl1POUNO TYPE ( ) ( lJ.. l ( ) ( ) ( ) ( ) UNITS ...,,,,.. Cun/ka ,~n/ka .. n/] un/ka un/] un/ka un/ 1 ··0 /ka .. n/ j .,nfkn N-nitrosodirrethvlamine JO/ () LI ~ I ,I - ls(2-chloroethvllether ch 1 ornoheno 1 ohenol ll:3-dichlorobenzene 4-dichlorobenzene 1,2-dichlorobenzene ts (2-ch loroi smrnnvl )ether xachloroethane -nitroso-di-n-nrnnvlamine Eobenzene horone trnnhenol 2.4-dirrethvlohenol o s (2-ch 1 oroethoxvl,rethane 4-dichloroohenol 1.2 4-trichlorobenzene • anhthalene I ~xachlorobutadiene • -ch l oro--01-Creso l hexachlorocvclnnPntadiene 14.6-trichlornnhenol chloronaohthalene acenaohthvlene nrrethvl ohthalate , 6-dinitrotoluene , acenanhthene ,, 4 dinitrnnhenol SO/JtoSO I, 4-dinitrotoluene /()l-:1:IO . nitrnnhenol ,0/11 • .::0 fl uorene 10/330 chlornnhenvlohenvlether I ethvl ohthalate J, 4,6-dinitro-o-cresol so /,;_c-o ·ohenvlamine /0/330 obenzene 4-brmr.nhenvlohenvlether ~xachlorobenzene ~ - >ntachlornnhenol so/11.:ro '' 1enanthrene J/1/:no ~, Qi;_ anthracene / ibutvl ohthalate / • I uoranthene V ' -s~ ,I:'.'... m1)L I -Estimated value. H,..o/SOIL- -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. The nurber t -Not analyzed. -Tentative identification. _ -On NRIJC List of Priority Pollutants. is the Mini= Detection Limit. mIJL ---- I I I g D D D u I I I BASE/NEUTRAL AND ACID EXTRACT ABLES <Xll1POOND nvrene benzidine butvl benzvl ohthalate benz(alanthracene chrvsene 3 3-dichlorobenzidine bis(2-<>thv1hexv1)ohtha1ate di-n-octvl ohthalate benzo(b)fluoranthene benzo(k)fluoranthene benzo(a)ovrene i ndeoo ( 1. 2 3-<:dl nvrene dibenzo(a,h)anthracene benzo(a h. ilnPrvlene aniline benzolC acid benzvl alcohol 4-ch loroani line dibenzofuran 2-rrethylnaohthalene 2-methvloheool 4-<nethvlohenol 2-nitroaniline 3-nitroani line 4-ni troani 1 i ne 2.4 5-trichlorochenol ff 7 J)~f' nP ,~ llA JC::.. J -Estimated value. K -Actual value is known L -Actual value is known U -Katerial was analyzed NA -Not analyzed. STATE LABORATORY OF l'UBUC IIEALlll P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS LAB NO l..lVJ/_ 70 (.jV I, .... ✓ ., FIELD# 11·;,.11)-.Sl "71-IVA-C:.°l TYPE ( ~ l (I.. ' l (. ) ( ) UNITS ~ .. n/kn ......,J un/knl un/ 1 ua/ka un/ 1 .. n/ka /0/~30 ~ ., •E,I~ 1...-,, 1,1.<o ',l - /0/330 £/4...- I A ➔OC . ,I, :l""' ...... J---' it.Ii'() SOI (IL.-- l/01330 / IO/.J.10 '¥ soht.<o //,, ",l) Ir II ACJ{) /,,' IA - I I I ,. ·1 I ' <oh,,.,co I.A ./ A- ... ✓ /() /_Z-U'I ~, S-ol,t.<o J I \I/ \ I '--------. -+-I-(-} r -1 I -- m:n1- H2.0I Soll.. to be less than value given. to be greater than value given. for but not detected. The nuroer is the Hinirrun Detection Limit. 1/ -Tentative identification. ~/ -On NHOC List of Priority Pollutants. ( ) ( ) .. n; 1 .. n/ka ""/1 ··"/ka I I I I I I I ~ I I I I I I I STATE LABORATORY OF PUBLIC HEALTH (!) PO BOX 28047 -306 N. WILMINGTON ST .• RALEIGH. NC 27611 ORGANIC CHEMICAL ANALYSIS PURGEABLECOMPOUNDS LAB NO qgzc.,v q82tt,z3 qg2.(pJ..5 qe,2.c.,27 qf3zlP2-'i C/f3203I FIELD NO CD-001-SL C!)-oo-Z-:il CD-003--'51.. {!()-oo '/-SL t/)-Oo5-:5 L CO·oo{p ·SL COMPOUND TYPE (:3 l ( 3 J (3 l ( 3J (0 J ( -3 l i1 MDL'f' (nob) ®ppm Bppm ----~ ~b ppm 8pm 9ppm (§) ppm CHLOROMETHANE ;l. ,() LL-LL U--I l I A IA VINYL CHLORIDE BROM OM ETHANE CHLOff.OETHA,.'VE ' I ' / TRICHLOROFLUOROMETHANE ' I ;z.t C. o.5 e- l,l·DICHLOROETHENE o,5 U-Ll-' I .. f ACETONE .2,0 /0. S c.,.) -'J.0,0 c; 43.o c; IODOMETHANE {),5 LL-IA /1 CARBON DISULFIDE METHYLENE CHLORIDE ACRYLONITRILE TRANS·l,2·DICHLOROETHENE METHYL-t-BUTYL-ETHER 1,1-DICHLOROETH.ANE ' I ISOPROPYL ETHER ' 7 ' I t--Y"OCP, /, q CIS·l,2-0ICHLOROETHENE ·r 2-BUTANONE ;2,0 LA-Jj. '7 ::r,t:. 3, I :r,J:. TETRAHYDROFURAN J,. u_ I J CHLOROFORM [),5 l. l, I-TRICHLOROETHANE CARBON TETRACHLORIDE . \ / BENZENE +race_ 1,2-DICHLOROETHANE ' / ' I 11 TRICHLOROETHENE {).&, S.B 1,2-DICHLOROPROPANE l-<...-, I • DIBROMOMETHANE ' I \ / \1/ .11 \ ~L \ / C-Possible lab contamination or background J - K - L - Estimated value L -,(,_ {) ,5 {) h Actual value is known to be less than value given. Tro.ce;.. I r p .. Actual value is known to be greater than value given. u - NA - 1/ - D - Material was analyzed for but not detected. The number is the Minimum Detection Limit. Not analyzed. Tentative identification. SAMPLE DILUTED. MDL'S DO NOT APPLY. DHHS 3065-1 (1/98) PURGCOM2.0RG I STATE LABORATORY OF PUBLIC HEALTH PO BOX 28047 -306 N. WILMINGTON ST .• RALEIGH. NC 27611 I ORGANIC CHEMICAL ANALYSIS PURGEABLE COMPOUNDS LAB NO '1821.PJ..I 962io23 98~i5 '162&2 7 '7'85lh::A C/62&5/ I FIELD NO f COMPOUND TYPE 131 13 ) r3 ) (."3) I q) ( . .,, ) ,tMDL~ Gppm (2:)ppm G)ppm 9ppm €)ppm 8ppm lnnb) I BROMODICHLOROMETHA."iE 0,5 lt.-LL U-I A I LL.-- CtS-1.3-DICHLOROPROPENE I 4-METHYL-2-PENTANONE TOLUENE I TRA..~S-1.3-DICHLOROPROPENE , \ I I 1, 1,2-TRlCHLOROETHANE " I TETRACHLOROETHENE , S.& 5&, I U-2-HEXA"lONE l,L I DIBROMOCHLOROMETHANE ETHYLENE DlBROMIDE I CHLOROBENZEXE l, l, l ,2-TETRACHLOROETHA."iE ETHYL BENZENE ' J I XYLENES ' / +r-{le,e.,, STYRENE I. O IA- I BROMOFORM (.,L... l, l ,2,2-TETRACHLOROETHA."iE I 1,2,3-TRICHLOROPROPA.."VE 1,4-DICHLOROBENZENE ' / I 1,2-DICHLOROBENZENE " f-rnrP , 1,2,-DIBROM0-3-CHLOROPROPANE :2,0 ' / ,7 U--' / \I/ \ I/ I il.,.Jrorn, L -::j <±7/r-i (-0 (-) A G c-) (-'.) di11r} o#ier /Jeak-5 , I I C -Possible lab contamination or background. I J -Estimated value K Actual value is known to be less than value given. L -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. The number is the Minimum Detection Limit. NA Not analyzed. I 1/ -Tentative identification. D -SAMPLE DILUTED. MDL'S DO NOT APPLY. DIIBS 3065-2 (1/98) PURGCOM2,0RG I I I I I ~ I I I I I I I I I I I I STATE LABORATORY OF PUBLIC HEALTH PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH, NC 27611 ORGANIC CHEMICAL ANALYSIS PURGEABLE COMPOUNDS LAB NO "1BUP33 FIELD NO CJJ-007-SL COMPOUND TYPE 13 l J, MDL+, / ppb ppm (nnb) - CHLOROMETHA."iE ;z,o u... VINYL CHLORIDE BROMOMETHANE CHLOROETHA.."iE TRICHLOROFLUOROMETHA.."iE ' I l,l•DICHLOROETHENE o,5 ACETONE ;2,0 IODOMETHA.."IB 0,5 CARBON DISULFIDE ' METHYLENE CHLORIDE ACRYLONITRILE TRANS-1,2-DICHLOROETHENE METJIYL.t-BUTYL-ETHER 1, l•DICHLOROETHANE ISOPROPYL ETHER CIS-1,2-DICHLOROETHENE ' I 2-BUTANONE ;2,0 TETRAHYDROFURAN J .. CHLOROFORM (),5 1, 1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE 1,2-DICHLOROPROPANE DIBROMOMETHANE , I \ r7 Possible lab contamination or background Estimated value K • L • qr:,,2h35 '1821P37 cv-006-sL C0-00'/-SL I 3 J ( 3 J ~ppm 9 ppb ppm u..... U- ' I -+r fl .. ., c.- . ' J ' -+-,,-r, r P +(ac0 J1 ,, \ / ' I 9BZ&39 9£324'-ll co-o l:Z ·SL C0-01'/ ·SI> ,..3 l r '-f l ~ppm ~ppm I I LL 'I (r, ,0 ""5,1'- U,_ .j--.ra.ce_ u__ J.,. J.5. '7 -l.)_., I 'f ' I u - Actual value is known to be less than value given. Actual value is known to be greater than value given. Material was analyzed for but not detected. The number Not analyzed. is the Minimum Detection Limit. NA· 1/ - D • Tentative identification. SAMPLE DILUTED. MDL'S DO NOT APPLY. I DHHS 3065-1 (l/98) C/82~'-l-3 Cl)-o 15-.:i) ( tf-1 c9 ppm /) ' J 8/,3L>:J" I I I (J' I., 15,3:r,1< /J ,I 167.4 lL o.&> lL J/ PURGCOM2.0RG I STATE LABORATORY OF PUBLIC HEALTH PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH, NC 27611 I ORGANIC CHEMICAL ANALYSIS PURGEABLECOMPOUNDS LAB NO cl62&>33 962&35 962&37 "182&:3q CJ82<o'f I 9B20i/3 I FIELD NO I COMPOUND TYPE ( 3 ) ( -:3i (3 ) ( 3) ( ,., ) ( '-{ ) ,l,MDL .. 9 ppm B ppm @ ppm 8ppm 9ppm Bppm (nnb) I BROMODJCHLOROMETHANE 0,5 LL L-L-l.,L LL I J 1 CIS-l,3-DICHLOROPROPENE I 4-METHYL-2-PENTA.."lONE 'I I / TOLUENE ;;. , lD ~6-fi> n TRA."iS-1,3-DICHLOROPROPE:'iE U-/J u 1.1,2-TRICHLOROETHANE I TETRACHLOROETHENE 2-HEXANONE I DIBROMOCHLOROMETHA.."iE ETHYLENE DIBROMIDE I / I CHLOROBENZENE 30/(p,5:r l, l, l ,2-TETRACHLOROETHAN'E ' I u._ ETHYL BENZENE ,e,.(o 3/.j-q. (.p I XYLENES tOl-/3,9' qq/e,,qT STYRENE I 1 I • I BROMOF'OR.'1: l, 1,2,2-TETRACHLOROETHANE I 1,2,3-TRICHLOROPROPANE ·, r \ I 1,4-DICHLOROBENZENE ).0,0 (p5,5 I 1,2-DICHLOROBENZENE , I q, I lttf-, 0 , 1,2,-DIBROM0-3-CHLOROPROPANE J.,0 ' I I / I \/ U-l,L... JI -1.,-~-L ~6 ff.1/?J 0-) ( _;_) (j)low G (-F) (+-) tII', ·,.,,vet I I one/ of.her pea/c:5 • I C -Possible lab contamination or background. I J~ -Estimated value Actual value is known to be less than value given. -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. The number is the Minimum Detection Limit. NA -Not analyzed. D -SAMPLE DILUTED. MDL'S DO NOT APPLY. I 1/ -Tentative identification. DIDI$ 3065-2 (1/98) PURGCOM2.ORG I I I I I I I II .I .1 i~ I II I I ' I I I ' ~ ~ STATE LABORATORY OF PUBLIC HEALTH PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH, NC 27611 ORGANIC CHEMICAL ANALYSIS PURGEABLECOMPOUNDS LAB NO qfjZ{p'-17 FIELD NO Cl)-ol1-5L COMPOUND TYPE ( 3 J ... MDL.., (nnb) £)ppm CHLOROMETHANE ;2,0 IJ VINYL CHLORIDE BROMOMETHANE CHLOROETHA..~E ' , TRICHLOROFLUOROMETHANE \ I O,Be- 1. l·DICHLOROETHENE o.5 lJ ACETONE ;2.,0 IODOMETHA.."IB D,5 CARBON DISULFIDE METHYLENE CHLORIDE ACRYLONITRil.E TRANS•l,2-DICHLOROETHENE METHYL-t·BtITTL-ETHER 1,1-DICHLOROETHANE ISOPROPYL ETHER CIS·l,2-DICHLOROETHENE ' I 2-BUTANONE :2,0 TETRAHYDROFURAN .l,, CHLOROFORM 0,5 l,l, I-TRICHLOROETHANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE 1,2-DICHLOROPROPANE 'I \ DIBROMOMETHANE Possible lab co.ntamination or background Estimated value K • 96Z& 'f C/ qe,2tp5/ W-011, ~L C'l)-o i'l ·5 L ( 3 ) (?, l ,,.-----)! ppb pm 8ppm / l U- ,I Id., 9 c,:r U-- ' / +race.- I - +ran, LL- " / -i-r,-, r~ LL. _\, 'I C/821.i,53 qg7-tp55 CD-oz,, 5L cD-022-S'- 13 l (3 l Bppm Bppm LL u.... I / + .--"' ,. p \ ( I /, 'f 'S I J ' , I +-r a.c e... I - \J / ' I u • NA - 1/ - D • Actual value is known to be less than value given. Actual value is known to be greater than value given. Material was analyzed for but not detected. The number Not analyzed. is the Minimum Detection Limit. Tentative identification. SAMPLE DILUTED. MDL'S DO NOT APPLY. D DHHS 3065-1 (1/98) @) q82w57 . Cf)-023-:SL ( 3) eppm / J 'I 0-8 ( I ,, PURGCOM2.ORG STATE LABORATORY OF PUBLIC HEALTH I PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH, NC 27611 I ORGANIC CHEMICAL ANALYSIS I PURGEABLECOMPOUNDS LAB NO C/82(p '-17 1B2u,L/C{ FIELD NO I COMPOUND TYPE 13) 13 ) ,t-MDL~ 8 ppm 8 ppm lnnb) I BROMODICHLOROMETHANE 0,5 11 u.....- CIS-1,3-DICHLOROPROPENE I 4-METHYL-2-PENTA..'IONE TOLUENE I TRA..'lS• l ,3-D ICH LO RO PROPE:VE 1, 1,2-TRlCHLOROETHA.."iE I TETRACHLOROETHENE 2-HEXA."'iONE •1 DIBROMOCHLOROMETHA..'VE ETHYLENE DIBROMIDE I CHLO RO BENZENE 1, 1.1,2-TETRACHUJROETHA."lE ETHYL BENZENE n XYLENES STYRENE H BROMOFORM u 1,1,2,2-TETRACHLOROETHANE H 1,2,3-TRICHLOROPROPANE 1,4-DICHLOROBENZENE 11 1,2-DICHLOROBE:VZENE , I ll l,2,-DIBROM0-3-CHLOROPROPANE J.,0 \ I ,/ i Ll. A ..-r1 r n,,. Jv, ,'1-<. (!J3/r-J G A ciad o+her Peaks , I C -Possible lab contamination or background. -Estimated value E J K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. 992&6( 13) eppm / I ' I ../-rcvP. I l J, I ,-; i, P I I ' I G 162fJi53 982&55 I '3 ) I 31 c9ppm Bppm lL l ' I -t-f"IVP C... / I . , - +-ro.ce._ ' , \ / . +n,,,., c.. ·, --p c.. . . , LL-/ J +ra.c.e..:. J~ D,!5 c.. +r,... ,.., _c.. I I I I '-I • I 8 (-) u -Material was analyzed for but not detected. The number NA -Not analyzed. is the Minimum Detection Limit. I) 1/ -Tentative identification. It D -SAMPLE DILUTED. MDL'S DO NOT APPLY. DlffiS 3065-2 ll/98) I CJ82.u57 I?) ;-;;;,)pm II / -1-,nrio "- ; I ,I/ +r-a.ce.. '- I l I ' C) PIJRGCOM2.0RG I I I I I ,, ~ I -I I I I I I I I I I I I STATE LABORATORY OF PUBLIC HEALTH PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH, NC 27611 ORGANIC CHEMICAL ANALYSIS PI/RGEABLE COMPOUNDS LAB NO 982(u6°i FIELD NO cP-Cf2'l-SiJ COMPOUND TYPE ( L\ ) .J, MDL ,l, (nnb) Appm CHLOROMETHA.YE ;l,O I.A- VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHA."iE ' I l, l·DICHLOROETHENE o.5 \ I ACETONE ;2.,0 '7, '7 -y,e, IODOMETHA.'IB {),5 /.A._, CARBON DISULFIDE METHYLENE CHLORIDE ACRYLONITRILE TRANS-1,2-DICHLOROETHENE METHYL-t-BlJTYL.-ETHER l, 1-DICHLOROETHANE ISOPROPYL ETHER CIS-1,2-DICHLOROETHENE \ I 2-Bt.rrANONE ;2,0 TETRAHYDROFURAN J,, CHLOROFORM {),5 1, l, I-TRICHLOROETHANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE l,2-DICHLOROPROPANE ' I \ I DIBROMOMETHANE C- J - Possible lab co.ntamination or background Estimated value 962~1 CD-o;l..5-SD ( '-\ ) @) ppm I l . ' I K - L - Actual value is known to be less than value given. Actual value is known to be greater than value given. 9'o2l<.>3 cD-o2<,,-SD ( '-I ) tp0pm I J ' I ts, I 6 J)(.. U- \ I 9BZ&(J)5 982<'.owT CD -o:33··'.)l dl-103-SL ( 3 ) ( 3) Bppm ~pm / J I I ./ ;/./' I I , l q,'f J°J / ' ,, (),5 \,,L, ' / J; u - NA - Material was analyzed for but not detected. The number is the Minimum Detection Limit. Not analyzed. 1/ -Tentative identification. D -SAMPLE DILUTED. MDL'S DO NOT APPLY. DHHS 3065-1 (l/98) 91:,2<'.ol? 9 cD-112.-5L ( 3) ~ppm tJ .,( PURGCOM2.ORG I STATE LABORATORY OF PUBLIC HEALTH PO BOX 28047 • 306 N. WILMINGTON ST., RALEIGH, NC 27611 I ORGANIC CHElrfiCAL ANALYSIS PURGEABLE COMPOUNDS LAB NO "!f,'.2<,,59 C/9Z4>Col qg,Upu,3 962lulu5 962&u,7 qe2<o&>9 I FIELD NO I COMPOUND TYPE ( '-l ) ( lj l ( '-( l ( :::, ) ( .3 l ( :3 l ,tMDL~ 8ppm ,,--:. @ppm €)ppm ® ppm 8ppm ppb ppm (nnb) I BROMODICHLOROMETHA."iE 0,5 LL I J / I u__ /J U- CIS-1,3-DICHLOROPROPENE I 4---METHYL-2-PENTANONE TOLUENE u TRANS-1,3-DICHLOROPROPENE ,/ l, 1,2-TRICHLOROETHA."iE I TETRACHLOROETHENE ~-'+ 2-HEXANONE " I DIBROMOCHLOROMETHANE . ETHYLENE DIBROMIDE ,, ' I ' I I CHLOROBENZENE +race c... .J-,-nn:, (. + ... ,.. ,p C. 1, 1, 1,2-TETRACHLOROETHA."iE I I -; I , ' ETHYL BENZENE .I/ ~'-J_ ,/ ~ XYLENES -1-i~ /JrP_ C., -1-ra.,.o_ c. +,r,,., rP C. fva.ce" STYRENE U-J JJ I I BROMOFORM 1,l,2,2·TETRACHLOROETHA."IB I 1,2,3-TRICHLOROPROPANE 1,4-DICHLOROBENZENE I 1,2-DICHLOROBENZENE 'f 1.2,-DIBROM0-3-CHLOROPROPANE J.,0 , I \, ,, 7 \I ' I \ / I Li.,,/ , rb.,.,,.,,,., fPJ/C) (-) ,-) ,-:-; (-') E) (-) a,1d <!J'iJWr /Jeaks , I C -Possibie lab contamination or background-Jl?(/i-c;,, A/el1'v rcrrh,m/nt:rf.ed ..:,a M./Jl,:s) I J -Estimated value + ·· T b K -Actual value is known to be less than value given. rttce::. LO. 5 PP L -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. The nwnber is the Minimum Detection Lim.it. NA -Not analyzed. 11/ -Tentative identification. D SAMPLE DILUTED. MDL'S DO NOT APPLY. DHHS 3065-2 (1/98) PURGCOM2.0RG I STATE LABORATORY OF PUBLIC HEALTH I PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH, NC 27611 I ORGANIC CHEMICAL ANALYSIS 5orry-l<>f+ PVRGEABLECOMPOUNDS LAB NO 98zw'11 I FIELD NO co-,z<.-SO I COMPOUND TYPE ( 4 ) ( J, MDL .j, ~ ppb ppm (nob) I CHLOROMETHA..-IB ;2,0 {I - VINYL CHLORIDE ~ BROM OM ETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE ' I [ l,l·DICHLOROETHENE o.5 I ACETONE ;2,0 IODOMETHANE D,5 CARBON DISULFIDE I METHYLENE CHLORIDE - ACRYLONITRILE I TRANS•l,2-DICHLOROETHENE METHYI,.t-BUTYL-ETHER I 1,1-DICHLOROETHA.."iE ISOPROPYL ETHER I CIS-1,2-DICHLOROETHENE ' I 2-BUTANONE ;2,0 TETRAHYDROFURAN J,, I CHLOROFORM D,fi 1,1,1-TRICHLOROETHANE I CARBON TETRACHLORIDE BENZENE I 1,2-DICHLOROETHANE TRICHLOROETHENE I 1,2-DICHLOROPROPANE . DIBROMOMETHANE 'I , I I C -Possible lab contamination or background J -Estimated value K -Actual value is known to be less than value given. ) ppm L -Actual value is known to be greater than value given. I U -Material was analyzed for but not detected. The number is NA -Not analyzed. !/ -Tentative identification. D -SAMPLE DILUTED. MDL'S DO NOT APPLY. I DHHS 3065-1 (1/98) ,/hl,~ ,ore o u:f I qr,;z(.45 £0-o/t.-5p ( ) ( 't ) ( ppb ppm eppm ppb I' . I ..J..rn,., J I \ I ;2.0 I I +rr,r,:, / J '1.r the Minimum Detection Limit. ) ( ) ppm ppb ppm PURGCOM2.ORG I STATE LABORATORY OF PUBLIC HEALTH PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH, NC 27611 I ORGANIC CHEMICAL ANALYSIS PURGEABLECOMPOUNDS LAB NO 982-LJ7/ qB2~'-/-5 I FIELD NO I COMPOUND TYPE ( 'i ) ( ) ( ) ( ,J ) ( ,tMDL~ /ppbjppm ppb ppm ppb ppm eppm ppb (nnb) I BROMODICHLOROMETHA.'IB 0,5' / J , /1 - CIS•l,3-DICHLOROPROPENE I 4-METHYL-2-PENTANONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1,1,2-TRICHLOROETHA.'iE ,/ g TETRACHLOROETHENE fra.ce... 2-HEXANONE 11- D DIBROMOCHLOROMETHA.~fE ETHYLENE DIBROMIDE '-I D CHLOROBENZENE I 3,-;i ,q 1, l, l ,2-TETRACHLOROETHA."(E lL ETHYL BENZENE /:20,S E XYLENES lf'71,O STYRENE 'J I BROMOFORM • 1, 1,2,2-TETRACHLOROETHANE I 1,2,3-TRICHLOROPROPA.'i"E ' I 1,4-DICHLOROBENZENE /.~ ' I ..5;;1.. 3 I 1,2-DICHLOROBENZENE 1,2,-DIBROM0-3-CHLOROPROPANE J.,O \ / v- Ll . .1 ..... -.1o-rhn,..,,-<. rrfYPJ (-) (+-) ~ , , i:1~1c1 o+her f}eal::'5 • C -Possible lab contamination or background. -Estimated value I J K • L Actual value is known Actual value is known Material was analyzed to be less than value given. to be greater than value given. for but not detected. The number u is tho Minimum Detection Limit. NA -Not analyzed. D -SAMPLE DILUTED. MDL'S DO NOT 11./ -Tentative identification. APPLY. DHHS 3065-2 (1/98) ) ( ) ppm ppb ppm PURGCOM2.0RG Ref 4 I I I I I I I I I LATITUD.E .AND LONGITUDE CALCULATION WORKSHEET 12 ···, LI USING ENGINEER'S SCALE (1/60) '· /·:) 0 0 0 _.... . ' s ITE NAME , __,,C=:c'-=-r-=-i'_,5,.,_J'.=e"-_,,_·_y=...,;....,.,µu.W\L\--"S_1,_,±~e-,~---cERcL Is , , Ne. O o o I . G, o (f ;i Su AKA: · ssID·: ---------------------------------- ADDRESS:. :L--"c)yc.,±r~ De. J 1/4 °';le (W 4-'Rt. is= cITY, rDxfncd -STATE, NC-zIP coDE, _______ _ sITE REFERENCE POINT: NE Corn fr tf-bY ;-/J,·n"'i,,, . USGS .QUAD KAP NAME: ___________ TOWNSHIP: (J N/S RANGE:. E/W SCALE: 1:24,000 . KAP. DATE: SECTION: 1/4 __ 1/4 1/4 KAP DATUM: 1927 1983 (CIRCLE ONE) KERIDIAN: COORDINATES FROM LOWE_R RIGHT (SOUTHEAST) CORNER OF 7. 5' KAP (attach photocopy): LONGITUDE: 12:.._ o 3.a·• ____ " LATITUDE: 3.u_o £. ' " . COORDINATES FRO!-i'--LOWER RIGHT (SOUTHEAST) CORNER OF 2. 5 ' GRID CELL: ' LONGITUDE: 1.'i_o 3S-: LATITUDE: 3/t__o U• 3.Q_u CALCULATIONS: LATITUDE (7.5' QUADRANGLE KAP) A) NUMBER OF RULER GRADUATIONS FROM LATITUDE GRID LINE TO'SITE REF POINT: B) MULTIPLY (A) BY 0.3304 TO CONVERT TO SECONDS: Jj_.__1_ .. C) EXPRESS lN MINUTES AND SECONDS (l'= 60"): · ZO. . LI _s_I_T_E_L_A_T_I_T_uD_E_= __ ~ __ a_.J.1_~· 5.Q __ ·==:_"_j CALCULATIONS: LONGITUDE (7.5' QUADRANGLE KAP) A) NUMBER_ OF RULER GRADUATIONS -~ROH RIGHT LONGITUDE LINE TO SITE REF POINT: ,i 0 _B) MULTIPLY (A) BY 0.3.304 TO CONVERT TO SECONDS: A X 0.3304 ·\ :\"' C) EXPRESS IN MINUTES< .AND'-SECONDS ( l' = 60"): -J_ • ~--•• D '·:,:D): ADD TO ·STARTIN_G .LONGITUDE: ·_1io~---_-_· _::_+ j_'. 2_•~~-~ -; ,,· <t . ·~ nd. J ~ •• s •• ,; •. J~ • . . . --... r-~~,': ;:_,j .)5_~TE LONGITuof: .. :.L.Jl.'0_.;3:J_ ' __ ·. __ · .. _ Ii , .. :· ... :,r:,··cc··c...:·._--,-'-,,I'-•,_. -,---,----==:---cc-'--,---'--.,...:..._';-_....J., II ...... DATE: • I E-10 i .• I I I I I I l;iJ ,, .. I I • I I I m m :I- I· I :! ll - ' ) SITE·. lUv-IB: . l /_, _ •020 r-•,, ~~1t1'-Ifft--""'"\J~~M1rr11-'-'~{37½~~-11-,4"'~'!J/,L1!-+-- )1 I, ,...,, ToPOGRAPH1c ,,.,AJ' QUADRANGLE NAME: cQ X focJ 7_f,}_(__.=--~----scALE: 1:,-:JX)). COORDIHA'~[S OF LOWER RJGHT-!-L•\J'ID COR:-,-,'ER Of 2.5-' :!NUTE GPJD:. LATITVOE:~0 _fJ_· 32· LONGITUDE -:2[, ~-- I ! I ' l i ! ; ' I I I I I I I I I I I I I Ref 6 -· . '-.. •. : ~-:'7;', .. ·-·,-.. ._ : · .. Y:ILA-_· >,-_..-._. f . __::_ __ • I f ., ,, .. . -. .. ' Environmental Science ~ervfces Administration Environmental Data Service linited States Department of Commerce, 1979, Climatic Atlas of the United States, ~ational Climatic Center, Asheville, NC. -- - - -- C s s NORTH CAROLINA - - --Not:.A1t'rL-A'-lJ.Jl')AL T:,1 /\ L ( / ivc,-t-.,:s) 0 - G -!!!!!!I !!!!!! == 44 (, -- - C 0 R G NOR TH CAROLINA ----- MEA-~ A>-JAJUAL.-L"-KE bv,t~Rlt-Tm>J (riv&tes) 0 ----- (, •liii" lliil llliiliir ..--------•---•---■----l!!!!l!!!I"'-•~---mr~··=m=--r:="""'liiiiiil-Siiiiiil •-llliiiiii l!llllliii .r:;s .• I ). ·. 11~:l',IIIT,\IEI\T IIF COMMEIICE .·,J""I ••. UcN1111.1-.. ~~,y u EATIIJ•:J: llllltE/,1, .I I / TECIINICAL l'Al»Eu NO. it.O JtAINFALL FUEQUENCY A'l'LAS OF 'l'IIE lJNl'l'Ell S'l'A'l'ES for Durulio11s fro111 30 Mi1111lc3 lo 21f, )lours aucl Return Periods fro111 ) lo ] 00 Years ,..,... ........ , DA\ IU M. llt:Jl!"otO'ft:Ut t __,.... .. 1 • ., SI_._._ S,....~ llt ............ :"or-nM._ I .. ,..__ ... t· I ••--llh----~t___..._S-,lrior \ PRCPERTY OF EPA FIT IV c;,,e __,_,:.C '0'"''\ '),"~ co"<:>', . \ -,_ \ 6() \\\C c.:,c.:i c,,-,<:>'. \ .,o'"" ; -------~ ~ ~ \ . ltl,,tl,ciJJL-/J~,\::-8:HVl:~ ,'it;.:, 'nµ5Q0 ~Y'.'.}:y::f_/4, \ _____s--lL~ o f -. ~ommerce - l9Gl 1, ----· .-;, ~-',-,' t~ . '-.c\. f ,--'J t ·1 I Te.c!1nical Pu ,er do. t, O \ ') g n I I I I I I I I I I ' State of North Carolina Department of Environment, Health and Natural Resources Division of Waste Management James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary William L. Meyer, Director October 8, 1996 Memorandum TO: FROM: Grover Nicholson David J. Lown~ an :n •-----. DEHNR RE: Personnel for Oversight of Removal Activities at Old A TC Refinery Site Wilmington, New Hanover County and the Cristcx Drum Dump (JFO/Channcl Master Site) Oxford, Granville County EPA will be doing removal activities at these two facilities sometime during the next two months. At Old ATC Refinery, Mike Taylor, EPA OSC, has requested that the NC Superfund Section have someone available for oversight activities, no sampling involved, beginning early in November. At the Cristex Drum Dump, Tony Moore, the EPA OSC, will begin trenching a drum dump sometime during this month. We should have someone present during the trenching. In reference to Old ATC Refinery, Mike Taylor called me yesterday and told me that an AOC was signed on for this site on August 2. The PRP is Axel Johnson, Inc. Geraghty and Miller (G&M) has been selected to prepare a workplan f<,r the removal of tanks, pipes, and drums. The tank and pipe removal has been subcontract,,d out to PetroClean (?) out of Pennsylvania. Two workplans have been prepared by G&M and rejected by EPA. Mike predicts that the removal activities will begin early in November. He has requested that the Superfund Section have personnel available, on a contingency basis, to do oversight during the removal. A geophysical survey was conducted at the Cristex Drum Dump in July 1996. Tony Moore talked to me on the phone yesterday. He said that the survey was inconclusive that trenching would be done sometime during this month. Tony is in the process of arranging for a backhoe to do the work and will contact me when he is ready to proceed. Because of my work load, I will not be able to be in the field during the trenching. cc: Pat DeRosa P.O. Box 27687, Raleigh, North Carolina 27611-7687 Voice 919-733-4996 FAX 919-715-3605 An Equal Opportunity Affirmative Action Employer 50% recycled/10"/o post-consumer paper I I D D I I I I I I I I I I 'I ,) I --- ---- -- - - -1!!!!11 1!!11:1 == 1 owe DA .1JAN96 j PR JCT NO.: NC0202.100 I FILE NO.: CHANNEL I DRA'MNC: SI TE2 l CHECKED: t~. SHE TTY I APPROVED: L. MORETZ "C1UIOIC(; ICCM'Ttl f"QJIII: 1-l "~-""' 1"2. .4 ..... GERAGHTY A.,-& MILLER, INC. .... Environmental Senrices ORUM DUMP , , ~~CRITE ', ' ' "' -----_, -------_;;;,-'--)--- 0 300 F[(T PROPOSED PUMPING WELL LOCATIONS JFD ELECTRONICS/CHANNEL MASTER OXFORD, NORTH CAROLINA == liiiiiil liiiiil I DRAFTER: A. Wr, ... iN = -)(-X-X-X-F"ENCE CULVERT -. --OR>,INAC( CREO:: ----~RTY LINE ~ TREE LINC ""'-"""' ·--= PROPOSED RECCNERY WOl. FIGURE 5-1 '· iiii m3] From: Ken Mallary 4/30/96 3:29PM (1687 bytes: 25 ln) To: Terry Stilman . 1fC: Ken Mallary, Cindy Gurley 11ubject: Buried Drums near JFD Electronics/Channel Master Site - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -Message Contents - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - D n D I I I I I I I I I I I I Hi Terry - I don't think I've met you. I'm an RPM in the North Superfund Branch and I wanted to inform the RAT Pack about a situation in Oxford, Granville County, North Carolina. Several years ago, while RD fieldwork was being conducted at the Channel Master Superfund Site, numerous buried and partially buried drums were discovered in a semi-wooded area behind an abandoned textile facility named Cristex. I don't know what the drums contain or how many drums are present (I would guestimate 30-100 drums). The area where the drums are buried is not fenced and is accessible to anyone. We have tried to locate the past owners/operators of the facility to no avail. Since the discovery of the drums, I've assumed that the PRPs for the Channel Master site were attempting to track down the former operators of Cristex -but I found out yesterday that they are not. The Superfund Section of the North Carolina Department of Environment, Health, and Natural Resources has asked if EERB would be willing to look into this matter. Could you bring this up with the RAT Pack and let me know if EERB has the manpower to address this situation in the near future? Please let me know if you need more information. I'm at X2038. PAV l I:> Law ..I ' N-c.. DH t-J\2. 'i t '1. -7 s 3 -'2. 'o o I 1r '?, 4-"j g D 0 u I I I I I I I I I I I August 23. 1996 De·Lymoneus Moore On-Scene Coordinawr U.S. Environmental Protection Agency Region 4 Emergency Response and Removal Branch :;4s C"unland S1ree1 1\tlanw. Georgia 30365 SUBJECT: Geophysical Report -Cristcx Drnm Site EPA Contract No. 6S-W5-0021 TDD No. 04-%06-:l00i Dear Mr. Moore: PRC Environmental Management, Inc. Gwinnett Corporate Center 1750 Corporate Drive Suite 735 Norcross, GA 30093 770-935-1542 Fax 770-935-9049 PRC PRC Environrne111al Managcmem. Inc. (PRC). has completed the geophysical survey c,,,1duc1ed al tile Cris1ex Drum Site located in Oxford. Granville Coumy. Nonh Carolina. The geophysiral report containing any anomalies detected is enclosed. If , . .,u have any questions. or need addi1iona! int"orrna1ion. please call rne al 1770) 717-2300 m Jack Siegel at 1770) 717-2343. [nclosur~ Douglas Thompson. Projl.'.ct Offic~r {L,.:ttcr \lilly) Jack G. Siegel. START Mcrnbcr (Lcucr Ouly) START Files I I -. g 0 D E I I I I I I I I I I I I MEMORANDUM TO: FROM: THRU: SUBJECT: DATE: SITUATION De'Lymoneus Moore On-Scene Coordinator, U.S. Environ111ental Protection Agency Region 4 .lack Siegel Superfund Technical Assess111cnt and Response Tca111 Steve Pierce Superfund Technical Asscss111e111 ancl Response Tea111 Leader Geophysical Survey Report -Cristex Drum Oxford. Granville Coumy. North Carolina TDD No. 04-9606-0007 August 23. 1996 Uncler the provisions of Technical Direction Document (TDD) No. 04-9606-0007. the U.S. Environmental Protection Agency (EPA) Region 4 tasked PRC Environmental Management. Inc. (PRC). Superfund Technical Assessmem and Response Tca111 (ST ART) to conduct a geophysical survey and provide a su111111ary report. The geophysical survey was conducted within a fenced. 1.5-acrc area located behind the for111er Cristex facility in Oxford. North Carolina. The North Carolina Department of Environ111ental Health and Natural Resources (NC DEHNR) requested Region 4 EPA involvemem afcer confir111ing that several empty dru111s were scattered at the site and that additional dru111s of potentially hazardous 111aterial may be buried under on-site debris 111ounds. Figure shows the general site location. In addition to a copy of lognotes and raw data (see Appendix A) and a list of witnesses (see Appendix 13). the Response Cost Managemem System (RCMS 1900-55) cost tracking inl'ormation (see Appendix C) is included following the text portion of tliis report. as requested. CRISTEX DRUM OXFORD, GRANVILLE COUNTY, NORTH CAROLfNA TDD NO. 0-1-9606-0007 N ·1 1 I g 0 D D I I I I I I I I I I I I BACKGROUND During the monitoring well installation phase of an unrelated remedial investigation at an adjacelll property (Channel Masters). several drums were obser·ved in a sparsely wooded to overgrown plot of land behind the Cris1ex facility. The property is owned by Mr. John Nelms. The abandoned drum sighting was reported 10 NC DEHNR. which in turn requested EPA assistance 10 inves1iga1e 1he po:-sihility of aJditional buried drums at the site. SUMMARY i\1 ahou1 I 330 hours on July I, 1996. START members Siegel and Neal departed the Region 4 START office fur Raleigh. North Carolina. 10 meet with the s1a1e represen1a1ive. Mr. Dave Lown. 1he next morning: Mr. Lown planned 10 accompany ST ART during the geophysical survey. On Julv 2. 1996. START personnel and Mr. Lown left Raleigh and arrived al the Cris1ex Drum site a1 about 0800 hours. Figure 2 shows the site location. Upon arrival. a brief visual survey was condu<.:ted. with the following observations: • Several rusted. 55-gallon drums were ~cattered along the rree line outside nr tile area to he investigated: no labels. or residues were visible in or on any of the drums. • • • The terrain was uneven. with several mounds of construction debris suspected of concealing buried drums. lJpon closer inspection. some of the mounds contained concrete ruhhle and corrugated metal: drums were ohserved through a crevice between concrere blocks at one of the mounds. The site covered about 1.5 acres and was overgrown with puison ivy anJ miler vegetation. The visual survey concluded al about 0900 hours. and START began clearing a baseline 10 esrahlish a 25-by 25-foot grid system. The baseline of the grid was cleared from the cemer post of a gale in 1he curved fence line (behind the Cris1ex facility) and terminated al a corner fence post 250 feel 1rencling eas1-nonheas1 towards 1he emrance of 1he site. Engineering tape was used 10 mark off 25-fooi intervals to establish ordinates "A" through "F" along the hase line: this line was designated ;1s zem axis." J ~ I 0 19]3 1:-0aLonr..e !<A,.ppi.n,;;' CRISTEX DRUM OXFORD, GRANVILLE COUNTY, NORTII CAROLINA TDD NO. 04-9606-0007 I I I I a D D R ~ I I I I I I I I I I A second line was cleared perpendicular lO the base line from the "D-ordinatc." The D-axis was marked off at 25-foot intervals lO establish ordinates O through 6. The 25 by 25-foot grids were cross-checked against the zero and D-axis lO confirm grid spacing. GEOPHYSICAL METHOD The geophysical survey at the Cristex Drum Site was conducted using the Geonics EM3 l -D noncontacting terrain conductivity meter. The geophysical survey was conducted with the EM3 l-D operated in both the quadrature phase and in-phase modes. The El'v13 l-D survey conducted in the quadrature phase mode was used to measure ground conductivity. A transminer at the leading end of the instrument induces circular eddy current loops that in turn generate a magnetic field in the underlying terrain. A receiver coil at the other end of the instrument intercepts a portion of the induced magnetic field. resulting in an output voltage that is directly proportional to the terrain conductivity. The voltage deflects a needle on the instrument that measures the conductivity in millimhos per meter. A second survey was conducted with the EM31-D operated in the in-phase mode. The in-phase mode is more sensitive to huried metallic objects. Negative deflections of the needle indicate buried metallic objects. Each phase of the geophysical survey was conducted as an independent survey. Readings were recorded at each node (or coordinate). The collected data was manually entered into a Lotus spread sheet. then electronically transferred imo Surfer for statistical analysis. The contours generated by Surfer were then imported into AulOCad Release 12 and overlain 01110 a scaled grid of the site. GEOPHYSICAL RESULTS The result of both quadrature phase and in-phase surveys produced anomalies that support the presence of metallic material (see Figures 3 and 4). However. because of the large amoums of surface debris (such as corrugated steel and concrete rubble) and uneven terrain. an accurate determination of the presence or absence of buried drums was not possible. 5 I I I I n D D m I I I I I I I I I I I The quadrature phase results indicated a relatively homogenous ground conductivity in the undismrhed northern areas where the background conductivity ranged between 14 and I 9 millimhos per merer. An area of nondetlecrion was detected near rhe mound of debris in the south corner of the site. Conducriviry readings between 22 to 30 millimhos per merer were detected at increasing levels towards the west. This area comained surface debris. uneven terrain. and the location at which drums were visually observed. The in-phase resuhs were relatively homogeneous throughout most of the site. except in the area of the mound in the south corner. where a maximum deflection was recorded (greater than 1000 millimhos/merer). A second location (B.0), near surface debris. also produced above background conductivity readings. CONCLUSION On July 2. I 996. START and a NC DEHNR represemarive conducted a geophysical survey at a suspected drum burial site located in Oxford. Nonh Carolina. Upon arrival. rhe sire was noticeably overgrown. Several empty drums were staged randomly outside a site perimeter fence. Although the uneven terrain made ir difficuh. ST ART established a 25-by 25-foor grid. The geophysical survey was conducted using the Geonics EM31-D noncomacring terrain conductivity merer in both rhe in- phase and quadrature phase modes. An anomaly plot was generated from data collected during each survey; however. rhe presence or absence of buried drums could nor be determined due 10 the large amoums of metallic surface debris. Despite the survey difficuhies. START did visually observe drums through a crevice between blocks in a mound of concrete rubble. START recommends additional investigation of rhe Crisrex Drum Sire. including the removal of surface debris. followed by trenching ro confirm or deny the presence of buried drums. 8 I I I I I g 0 E I I I I I I I I I I I '.:.◄--------' ◄ 6 s 5 8 4 3 2 MOUND 26 1/ :NI 6 • B C D E ~i-F . ~ 7 r~" , >< "' :-1----j ---~i-~ SCATTERED DRUMS ~ _...,...-i-111111111111111 ~---25 FEET , .... :-i..--- GATE 0 A CRISTEX DRUM l!Xfl!RD, GRANVILLE, NORTH CARIJUNA CONTOURS REPRESENT ELECTROMAGNETIC 1----T_DD_ND._0_4-_96_0_6-_0_00_1 __ ~ SURVEY USING AN EM31-D. DAT A VERE REDUCED USING SURFER 5.2, CONDUCTIVITY= MILLIMHOS/METER CONTOUR INTERVAL = 5 6 FIGURE 3 EK31 SURVEY -QIJADRA TURE PHASE MODE 111W: ENVIRIJNHENTAL MANAGEMENT, INC. I I I I m I g D E m I I I I I I I I I 00,__ ____ 68 6 5 4 8 3 0 2 MOUND 6 1/ 70 B C D E :-V-i-F ~ GATE 0 A >f FENCE"-._ ._.,,,.,..~ J "' ~_.,,,.,..~ j _.,,,.,..'1-_.,,,.,..'1-:..----"' SCATTERED DRUMS I -1.. _.,,,.,..-,.. 1111111111111 __.-::(_.,,,.,..i-_____..., -25 FEET _.,,,..i- CRISTEX DRUM OXFORD, GRANVILLE, NDRTH CAROLINA CONTOURS REPRESENT ELECTROMAGNETIC I----T_DD_N~_o_4-_9_6D_6-_0_00_1 __ ____, SURVEY USING AN EM31-D. DATA \v'ERE REDUCED. USING SURFER 5.2, CONDUCTIVITY= MILLIMHOS/METER CONTOUR INTERVAL = 50 7 FIGURE 4 EM31 SURVEY -IN-PHASE HDDE l1ieC ENVIRONMENTAL MANAGEMENT, INC. I I, I I I I I I I I n u H D D D D E E I RESOURCES Autodesk. Inc. 1992. t\utoCadd Release 12. DeLorme Mapping, 1993. MapExpert Version 2.0 for Windows. r:reepon. Maine. Golden Software. Inc. 1994. Surfer Version 5.2 for Windows. Golden Colorado. Geonics 1-imited. l'J94. Operating Manual for EM31-D Non-Comacting Terrain Conductivi1,· Meter. Missauga. Omario. June. APPENDIX A Copy of Lognotes and Raw Data 13 Witnesses C Response Cost Managemem System (RCMS 1900-55) 9 ' J I I I I I I m D u 0 D I I I E I I I I APPENDIX A COPY OF LOGNOTES AND RAW DATA (eight pages) , 'j __ .. ••-------~-----~----~ MEASUREMENT CONVERSIONS ICH CM IF YOU KNOW ,. MULTIPlY TO FIND BY LENGTH ' --inches 2.540 oontime\ors feel 30.480 centimeters yards 0.914 me1ers miles 1.609 k~omelers millimeters 0.039 inches centimeters 0.393 inches meters 3.260 ,oo, meters 1.093 yards kilomoters 0.621 miles WEIGHT """"' 28.350 g•.1ms ' --""'""' 0.453 kilograms grams 0.035 _., kilograms 2.204 pounds VOLUME 2 fluid ounces 29.573 mdhlltors p1nts 0.473 liters quar1s 0.946 htors gallons (U.S.) 3.765 liters milhli!ers 0.033 fluid ounces liters 1.056 Quarts 111ers 0.264 gallons (U.S.) ;p TEMPERATURE 3 I •c = ("F • 32) x .555 "f={"Cxl.8)+32 Decimals Mini• """°' !2!l2oJ m<l 1/16 .0052 1.5875 H8 .0104 3.1750 10== ' J/16 .0156 4.7625 ,, ,,. .0208 6.3500 '"' .0260 7.9350 11== 3'8 .0313 9.5250 112 0417 12.700 S18 .0521 15.875 •• .. ,,, .0625 19.050 718 .0729 .. 22.225 ,. .08JJ 25.400 2· .1667 50.600 3· .2500 76.200 ,, .3JJ3 101.60 s· .4167 127.00 14=== ,. .5000 152.40 ,. .5833 177.80 8' .6667 203.20 ' --9' .7500 228.60 10· .8333 254.00 ,,. .9167 279.40 11001 1.0000 304.80 1s== OJ..J-5-0olf/ Name C fl I 5 Ii f. i) ;Z // f"'\, S I Tl- () X'fOrlj) ; (,\.)(1.,,. } Address Phone ____________________ _ Project LEGAL DOCUMEl\lT DO NOT D!::STROY •Rite In the Rain• • a unique all•weather wriling sur1ace created to she~ water and to enhance the written image. Makes it possibfe to write sharp, legible field data in any kind of weather. a product ol J, L. DARLING CORPORATION TACOMA, WA 98421-3696 USA .. ------------------ --------!!!!5-,i,1!1111~""1!!!!~---fl!!!!!!!t--~::r-~=--=r-----lili'- / ' PAGE ' ,. CONTENTS REFERENCE DATE -'·-···-··· _rl:_5:__S_t:,J[_t;;__c;_ ------- ------------ -- - - i~fe;O_ ?7/i/l-r_,:;,/16f( ,Me.f tu'f_4_ _e'5c_ -[e_;_~-(-/l1.al,r l / /j_itJ' o __ . d';f [_Lz__ _ f~'J/?__ ___ _ )CJ _6,i_-r. 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I 'is /DO !7o J;_ s-,6 , oo 9~ £ t, ,B IO !'J go ~ t/ ,, , ' lo' ~o ,?-3 • ' /00 ~o • Field data shfft is an txtfflSlon of Geophysical Logbook ____ _ Location ---------- A-7 I I I I a D D E m I I I I I I I I I .I page J:.ot z_ EM FIELD DATA SHEET STATION .r /V /"II-~ 5 f, ptOl:if Instrument Conductivity X y Reading SCALE mmholm Comments . ;:::-2-,go IP v !?tJ ,::::. b f;)O /00 b'B -~ 5' • r,; )( /00 t-/t / b ,6-1 /,o/Y bi . .• • Field data shfft is an extfi!Slon of Geoph~cal Logbook ------ Location ----------- I I I I m g n D u m m I I I I I I I I APPENDIX 13 WITNESSES (one page) I I I D 0 D E I I I PRC Environme111al Managemenl. Inc. 1750 Corporate Drive. S1e. 735 Norcross. Georgia 30093 770-7 I 7 -2343 WITNESSES START members: .lack Siegel and Timo1hy Ne;1J Nonh Carolina Departmem of Environmental Health and Natural Resources 401 Oberlin Road. P.O. Box 27687 Raleigh. NC 27611-7687 9 I 9-733-2X0 I. Ext. 349 David Lown 13-1 I I I I I I I I I I I I I I I I I I - ' \ MEMO DATE: TO: FROM: SITE: November I, 1996 File Jeanette Stanley Environmental Chemist NC Superfund Section JFD Electronics/Channel Master (Cristex) NCO I 22 263 825 Oxford, Granville County, North Carolina On October 30, 1996, David Lown, Engineer, NC Superfund Section, and I visited the drum dump site behind the Cristex facility which is near the JFD Electronics/Channel Master NPL site. While there, we met Tony Moore, US EPA ERRB; PRC Start contractors Mike Collins and Justin Mehta; and equipment operators with "Inco", Johnny Baines and Albert Steele (919) 446-1174. David Lown and the Project Manager at the JFD Electronics site had previously noted the tops of buried drums in the area and ERRB had been requested to an do as,sessment of the area. Tony Moore order the excavation of two intersecting ditches in the drum area. In the first ditch, no waste was noted and it was backfilled. In the second ditch, drums were noted. Two contained a tar- like material and another contained a liquid that, when disturbed by the backhoe, spilled into the ditch. Tony ceased excavation, and containerized as much of the waste material as possible in a drum. I took photographs of this activity. I photographed the top of a buried drum and the mound area prior to the excavation and the excavation activities. These photographs are attached. We then attempted to contact the property owner of the Cristex property in order to get permission to place a roll off box inside the flat, fenced area. David and I found the advertised number for the real tor handling the property on a sign in front of the Cristex facility -"Lucas & Beach" (800) 420-1817. David called this number, left a message and we left the site. In a subsequent telephone conversation between David Lown and Tony Moore, David informed me that a "Faze"(?) Morrisey, Cristex property caretaker 690-030 I had let the US EPA place a roll off box inside the fenced area on the Cristex property. The owner of the property is George Christensen (908) 458-8073. I called Tony Moore today, November 1, 1996. He said that the waste generated by the assessment was contained in the roll off box and they are awaiting analytical results. I asked ifthere was an action memo or any written authorization for this investigation,. Tony said that this was an assessment and that no written authorization is generated for an assessment. There will be an action memo for the removal action. Ref 9 !I w ,\ I ,, 1 I I I I I I I I I I ! I I I I I I I February 25. 1997 Mr. Tony Moore On-Scene Coordinator U.S. Environmental Protection Agency I 00 Alabama Street, SW 11th Floor Atlama. GA 30303 Subject: Cristex Drum Site Oxford, Granville County, North Carolina TDD No. 04-9610-0016 Dear Mr. Moore: PRC Environmental Management, Inc. Gwinnett Corporate Center 1750 Corporate Drive SuHe 735 Norcross, GA 30093 770-935-1542 Fax 770-935-9049 Enclosed is a summary of activities that the PRC Environmemal Managemem. Inc. (PRC) Superfund Technical Assessmem and Response Team (ST ART) performed at the Cristex Drum Site in Oxford, Granville Coumy. North Carolina. 011 October 30 -31. 1996. Also enclosed are site logbook notes. a photograph log, and site diagrams. If you have any questions concerning the summary. please call me at (770) 717-2300 or contact Justin Mehta at (770) 717-2344. Sincerelv. -·----.---~;-.,,,~-:.f/[--~-·--.. '\, .. /" \. _1 •. _-. _ _... ·---• .. :. _.<-.... ···- R. Steve Pierce START Leader Enclosures cc: Douglas Thompson, EPA Project Officer (letter only) Justin Mehta, Project Manager START File 11 I I I I I I I I I I I I I I I I I ' CRISTEX DRUM SITE OXFORD, GRANVILLE COUNTY, NORTH CAROLINA TDD No. 04-9610-0016 BACKGROUND The Cristex Corporation (Cristex) is a 1.5-acre facility located in Oxford. Granville County, North Carolina (Figures I and 2). Cristex is now leased to various companies to be used as storage space. File material indicates that the North Carolina Department ·of Environmental Health and Natural Resources (NCDEHNR) notified the U.S. Environmental Protection Agency (EPA) Region 4, of the possible presence of drums at the Cristex site. EPA tasked the Superfund Technical Assessment and Response Team (START) to mobilize to the site and conduct a geophysical survey. START and NCDEHNR conducted a geophysical survey on July 2. I 996, at the site and noted the following: (a) that several rusted, 55-gallon drums were scattered along the tree line outside the area that was to be investigated during the geophysical survey, (b) that the terrain was uneven with several mounds of construction debris suspected of concealing drums, and (c) that the mounds contained rubble. corrugated metal. and drums. SITE ACTIVITIES On October 30, 1996, START returned to the site with its subcontractor, !NCO, to conduct a second site investigation. START initially performed a visual reconnaissance to determine the exact suspect area and also the best access route to the area. In Level B personal protective equipment (PPE) and equipped with a radiation meter, Photoionization Detector, Organic Vapor Analyzer, Combustible-gas Indicator, and a Soil Gas Probe, START began to examine the mounds of suspected rubble to determine subsurface conditions. No readings were registered. !NCO (who provided the backhoe, dump truck. and air cylinders) and ST ART prepared the backhoe for excavation of trench I (Figure 3). Still in Level B PPE, START monitored the excavation of trench· I, during which no drums were discovered: trench I was then backfilled. The backhoe was repositioned in order to dig trench 2 (Figure 3), where START and !NCO discovered drums containing a black tar-like substance. ST ART and !NCO stopped excavating and placed the drums on Visqueen along one side of trench 2 and sampled the contents. When trencl1ing continued, another drum was discovered and acciclently cracked open by the backhoe. A light-colored oil spilled into the trench. Once again excavation was stopped and START sampled the material. Additionally START performed HAZCA T field screening analysis on samples of both, the tar-like and light-color oil substances. Initial results showed both substances to be combustible/flammable and potentially to contain chlorinated compounds. The On-Scene Coordinator (OSC) decided that a roll-off box would be needed to contain the drums and contaminated soil. Trench 2 was then covered with Visqueen and the site was secured. START and !NCO arrived on site at 8:00 a.m. Wednesday, October 31, 1996, and the roll-off box arrived at 9:00 a.m. The box was then positioned by the backhoe and loaded with drums and contaminated soil. !NCO secured the roll-off box, and the trench was re-covered with Visqueen and secured with soil. The backhoe was pressure-washed, and the site was then secured with caution tape. The site and the roll-off box have been turned over to OHM Remediation Incorporated (OHM), an Emergency Response Contracting Service contractor. OHM will continue the cleanup activities, as well as the removal of drums and contaminated soil. Future actions will be determined by the OSC. r--- - -- - - -- - ____ , - - - I!' N t I/-------~----------...,._:=:==.-- CRISTEX DRUM SITE -'\, .. , .. , ."-·,, ',<- OXFORD. GRANVILLE COUNTY. NORTH CAROLINA TDD No. 04-% I 0-00 I 6 ,\,,\tfl ~/..\,.~. ~~--..;.·-~G,p.'" FIGURE 2 ~ SITE LOCATION MAP ~ =---..... --------------~=~~~ NORTH CAROLINA CRISTEX DRUM SITE OXFORD. GRANVILLE COUNTY. NORTH CAROLINA TDD No. 0-1-9610-0016 fi D D 0 I g I I I I I I I I I I '•·· i Subject: Location: Orientation: TDD No: Photographer: OFFICIAL PHOTOGRAPH No. 1 U.S. ENVIRONMENTAL PROTECTION AGENCY View of START and INCO initiating the digging of trench one. Cristex Drum Site Investigation Oxford, Granville County, North Carolina North 04-96 I 0-00 I 6 Date: October 30, I 996 Mike Collins, ST ART Witness: Justin Mehta, ST ART A-1 0 I I I I I I I I I I I I I Subject: Location: Orientation: TDD No: Photographer: OFFICIAL PHOTOGRAPH No. 2 U.S. ENVIRONMENTAL PROTECTION AGENCY View of START member using a Photoionization Detector (PIO) testing for organic vapors, in trench one. Cristex Drum Site Investigation Oxford, Granville County, North Carolina North 04-9610-0016 Date: October 30, 1996 Mike Collins, ST ART Witness: Justin Mehta, ST ART A-2 I I I I I I I l ,, B II Subject: Location: Orientation: . TDD No: Photographer : OFFICIAL PHOTOGRA P H No. 3 U.S. ENVIRONM E N T A L PROTECTIO N AGENCY View of START and INCO initiating the digging of trench two. Cristex Drum Site Investigation Oxford, Granville County, North Carolina Southwest 04-9610-0016 Date: October 30, 1996 Mike Collins, START Witness: Justin Mehta, ST ART A-3 1 E E 0 D u a I a I I I I I I I I •• ( Subject: Location: Orientation: TDD No: Photographer: OFFICIAL PHOTOGRAPH No. 4 U.S. ENVIRONMENTAL PROTECTION AGENCY The first drum that was uncovered; the drum was empty. Cristex Drum Site Investigation Oxford, Granville County, North Carolina Southwest 04-9610-0016 Date: October 30, 1996 Mike Collins, START Witness: Justin Mehta, ST ART A-4 0 0 D 0 0 n 0 D D D 0 D D D 0 D 0 "U ( Subject: Location: Orientation: TDD No: Photographer: OFFICIAL PHOTOGRAPH No.5 U.S. ENVIRONMENTAL PROTECTION AGENCY The first appearance of the tar-like substance that was found in trench two. Cristex Drum Site Investigation Oxford, Granville County, North Carolina Southwest 04-9610-0016 Date: October 30, 1996 Mike Collins, ST ART Witness: Justin Mehta, ST ART A-5 0 u E I I I I I I I I I I I Subject: Location: Orientation: TDD No: Photographer: OFFICIAL PHOTOGRAPH No.6 U.S. ENVIRONMENTAL PROTECTION AGENCY The first drum of the tar-like substance that was uncovered from trench two. Cristex Drum Site Investigation Oxford, Granville County, North Carolina Southeast 04-9610-00 I 6 Date: October 30, 1996 Mike Collins, ST ART Witness: Justin Mehta, ST ART A-6 I I I I I a 0 D I m I I I I I I I -. / Subject: Location: Orientation: TDD No: Photographer: OFFICIAL PHOTOGRAPH No. 7 U.S. ENVIRONMENTAL PROTECTION AGENCY The first drum that was removed from trench two, with the tar-like substance being released from the drum. Cristex Drum Site Investigation Oxford, Granville County, North Carolina Southeast 04-9610-0016 Date: October 30, 1996 Mike Collins, ST ART Witness: Justin Mehta, START A-7 I D D D m I I I I I I I I I I ll Subject: Location: Orientation: TDD No: Photographer: OFFICIAL PHOTOGRAPH No. 8 U.S. ENVIRONMENTAL PROTECTION AGENCY The drum, from trench two, after it has been laid out on plastic. Cristex Drum Site Investigation Oxford, Granville County, North Carolina Southeast 04-96 I 0-00 I 6 Date: October 30, 1996 Mike Collins, ST ART Witness: Justin Mehta, START A-8 I I I m n n D m I I I I I I I I I Subject: Location: Orientation: TDD No: Photographer: OFFICIAL PHOTOGRAPH No. 9 U.S. ENVIRONMENTAL PROTECTION AGENCY View of light-color oil which poured into the bottom of trench two. Cristex Drum Site Investigation Oxford, Granville County, North Carolina Southwest 04-9610-0016 Date: October 30, I 996 Mike Collins, ST ART Witness: Justin Mehta, START A-9 I n u E E I I I I I I I I I I Subject: Location: Orientation: TDD No: Photographer: OFFICIAL PHOTOGRAPH No. 10 U.S. ENVIRONMENTAL PROTECTION AGENCY View of additional drums buried just beneath the surface of trench two. Cristex Drum Site Investigation Oxford, Granville County, North Carolina Southeast 04-9610-0016 Date: October 30, 1996 Mike Collins, START Witness: Justin Mehta, ST ART A-10 I I I I I I n D m I I I I I I I I Subject: Location: Orientation: TDD No: Photographer: OFFICIAL PHOTOGRAPH No. 11 U.S. ENVIRONMENTAL PROTECTION AGENCY View of Chlor-N-Oil test results. Results show the machine oil contains greater than 50 ppm of PCBs. Cristex Drum Site Investigation Oxford, Granville County, North Carolina Southeast 04-9610-0016 Date: October 30, 1996 Mike Collins, START Witness: Justin Mehta, START A-11 I I I I I I I I I I I I I I I I I I .1 Subject: Location: Orientation: TDD No: Photographer: OFFICIAL PHOTOGRAPH No. 12 U.S. ENVIRONMENTAL PROTECTION AGENCY View of the roll-off box. Cristex Drum Site Investigation Oxford, Granville County, North Carolina Northwest 04-96 I 0-00 I 6 Date: October 30, I 996 Mike Collins, START Witness: Justin Mehta, START A-12 CM 1 -- ·-- 11== 14== MEASUREMENT CONVERSIONS lFYOU KNOW LENGTH inches leet yards miles millimeters centimeters me1ers rm!ters kilome1ers WEIGHT ounces pounds grams kilograms VOLUME lluid ounces pints QlSilrtS gallons (U.S.) milliliters lilers h1ers TEMPERATURE MULTIPLY BY 2.540 30.480 0.914 1.609 0.039 0.393 3.280 1.093 0.621 28.350 0.4S3 0.035 2.204 29.573 0.473 0.946 3.785 0.033 1.056 0.264 "C .. (°F · 32) 1t .555 •F: {"C x 1.8) + 32 1116 118 3116 1,. 5116 3'8 112 518 314 718 1· 2· ,. .. s· ,. 1· ,. ,. 10' 11" 11001 Decimals <>l.J20I .0052 .0104 .0156 .0208 .0260 .0313 .0417 .0521 .0625 .0729 .0833 .1667 .2500 .3333 .4167 .5000 .5833 .6667 .7500 .8333 .9167 1.0000 TO FIND centimeters centimeters meters kilomelers inches inches lool yards ~,., grams kilograms ounces pound, milliliters lders liters filers nuid ounces quart, gallons (U.S.) Milli• -1.5875 3.1750 4.7625 6.3500 7.9350 9.5250 12.700 15.875 19.050 22.225 25.400 SO.BOO 76.200 101.60 127.00 152.40 177.80 203.20 228.60 254.00 279.40 30<.80 Ot./· ~-010S tE!AL DOCUMENT Name oa !\IQT pc-srPOY I) ® ALL-WEATHER• WRITING PAPER Address ____________________ _ Phone ______________________ _ Project •Rite In the Rain• • a unique all-weather writing surface created to shed water and to enhance the written image. Makes it possible to write sharp, legible field data in any kind of weather. a product of J. L. DARLING CORPORATION TACOMA. WA 98421-3696 USA ceNTENTS PAGE REFERENCE DATE tl./ov -D~c--+ ":>TA.I\• ,,,JI.-~--J:,. G--cc.,...\.•"', A.) c.. c,J"c.-_ ----~ () ,.-¥.-i.. IJ <:.. - z zoo -. ~,-,.-.~ ~ \4.,-1~\. --~ c;z:2_ ~ . .. Oc,&,w ~o , 199 6 _ 07a> __ A,\\; .... ~ ~\.¼:... M<:d · ..... ~y c-,f \\o-+~l... . A.,.,....{.;1 0-.. c. o "e• 1:::-; k. ~ <i:s-+<-• ,j.o,t ocio G.~,,.:t'~~~ co..~ .... ~ ..,, / D~C... . . •-~<L w ,· .,__ p~c::..--r ... . Otk) ___ T..,._,~ .. c,..l-<-;-,.....0 0.:,:-8'2.-l'Jt~ \...,,"<'-.\ ·. _ G,~ .... -t-~ ~ w ( -Sc.\...~"'( &..·,"._,. --~~--~-~' 0---.. fl..., --.. -. _-__ -_..:----- . &o:, .... ..,,, i11.~-.c.o~~ ..1r\...t ei ..... 1c-1.o ... . \I -r ~ :-t~ t,( c,r,:. ~ ~ ~ ~ . _______ ~_<Al _e.,.,-,.~ __ ....e-h..1 .. (. O?l/5'. _6....,IC:"'-oc. ! b"'4' ~I( c,.''-f"i~ 04 .. ~-. G,~.,, ~ __ e,,,N 1-1 .. 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Joel Shields with OHM Corporation reported to me that they had found 25 buried drums with contents and I'l 2 empty drums scattered about the property. Joel reported that a driver for the Oxford Oil Co. had told him that the large vertical tank had a broken valve a few years ago. The tank leaked and flowed into the lagoon. Joel said that the Oil Co. driver reported that he had noticed a line of "Four Seasons" Truck at the facility after the spill. Joel did not know the driver's name. , Tony Moore, US EPAERRB arrived at the removal site around 1015. He said that the drums they have removed were found to have been carefully placed in the hole prior to burial. Whoever • placed the drums in the hole had placed plastic on the ground before placing the drums in the hole. After the drums were covered with soil, vegetation had grown and there were weeds and brambles growing on top. Tony said that the drums contained at least four types of materials . Mr. Moore said he had done some research on former operators of the Cristex facility. IMI (Irving Meltzer) and Steinfeld Mills were two of the former operators. Mr. Munn, facility manager, was at the facility when I was there and I asked him some questions. He said that the area behind the fence (where the drums were buried) was accessible from the road. He said that he knew that there were many empty drums in the area. He said that the other chain link fence built on the other side , of the Cristex fence (leaving a driveway width access to the drum burial area), had been built in recent years. Mr. Munn gave me the corporate address: Cristex Corporation P. 0. Box 527 Allenwood, NJ 08720-0527 (908)458-8073 Mr. Munn said that the President and owner is Mr. George Cristensen (908) 499-7463. E I I I .I I I I I I I I I MEMO DATE: SITE 1,-io/ January )-5', I 998 Cristex Drum site .Mr. Munn said that the building was built in 1965. Facility operations never changed, but the owners of the facility had changed several times over the years. The facility made fricot. The plant did knitting, dyeing and finishing of the tricot. I then walked around the facility and noted four drums on the front south comer and a line from a tank that emptied into a ditch. A drawing of this area is shown below. Three drums had readable labels. One drum was labeled Betz Entec 382 and another was labeled Cristex Corp. Inc. Dr., Oxford, NC. Another was labeled "solvonics" LG 43 and had the following logo on it: Drum logo I attempted to photograph the drums and several other areas around the facility, but the camera was not working properly. Two photographs were taken, valving and signage at the base of the vertical tanks and the lagoon. _ Mr. Moore and l then went to the offices for the City of Oxford. We reviewed files and copied many of these files. We met with Mr. Jesse Sullins, Jr., P. E., City Engineer. He assisted us with locating files and provided some information. He said that in 1986, Cristex was no longer in operation. He also said that a Mr. William Bruce was a Vice President of manufacturing. Mr. Moore and l return to the site and I took tv.o photographs of the two vertical tanks, roll off boxes and overpackcd drums. Mr. Moore said that Cristex had given EPA permission to store these at this location while waiting for removal. In a subsequent discussion, Mr. Moore said that the staged materials w,;re removed from this location sometime in March I 997. He also said that all stockpiled soils were found to not be hazardous materials and were used to backfill the pits. l .. ·----------'----------- -----___ I ____ ---_, __ - 1---1 _______ _I ___ ·------. ·-- 1 I , .. I __ : __ --~-· L -~-~ -. ~LI= ~ ~=' ~~~1-.· .· I~~------1 I i ___ ! --~ -----I ··1· --------- - I i I I I . ! ______ / ___ . ------· _. 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BACKGROUND Site No.: Delivery Order No.: Response Authority: NRC# ERNS No.: CERCLIS No. : NPL Status: State Notification: Action Memorandum Status: Start Date: Completion Date: III. SITE INFORMATION A. Incident Category March 31, 1997 Cristex Drum Site, Oxford, Granville County, North Carolina De'Lyntoneus Moore, OSC First and Final A468 4003-F4-060 CERCLA N/A N/A N/A NON-NPL NC DEHNR Notified Signed December 3, January 16, 1997 March 28, 1997 1996 CERCLA Incident Category: Other-Material dumped by Inactive Production Facility B. Site Description 1. Site Location The Cristex Drum Site is located in an light industrial park in { Oxford, Granville County, North Carolina. The site is an unauthorized burial ground for discarded waste material. It is suspected that the drums were buried in the area by the occupants._ of the Cristex facility. The burial date is suspected to be around .... This coincides with a documented spill incident at the Cristex Facility. The Site was identified the by North Carolina Department of Health, Environment, and Natural Resources (DEHNR) through their work at an adjacent NPL Site. Drums are scattered in two distinct clusters with individual drums radiating from each cluster. Some drums were partially or completely buried. The condition of the drums ranges from intact to extremely deteriorated. The location is highly accessible and adjoins a nearby a~artment complex. Ownership of the Site is unknown. The area appears to be located within the right-of way of the local utility company. Approximately 1,000 residents live within a two mile radius of the Site. 2. Description of threat E D C. Preliminary Assessment/ Site Inspection Results On May 2,1996, North Carolina DEHNR referred the site to region 4 ERRB. OSC mobilized to the site on May 14, 1996 to perform a walk-through with the NC DEHNR Officials. The OSC documented two distinct drum clusters with individual drums radiating from each cluster. Some drums are partially or completely buried. It was suspected that more drums are buried under the visible drum clusters. The condition of the drums ranges from intact to extremely deteriorated. A geophysical survey was arranged for July 1~2, 1996; to ascertain the presence of buried drums at the site. The survey indicated several anomalies in the area of concern. Invasive trenching was performed in the area of concern on October 30-November 1,1996. Several drums were uncovered in this survey. Due to the deteriorated condition of the drums, three of these drums ruptured during the operation. Field test revealed that the drums may contain a chlorinated compound. This finding was the basis of the subsequent removal action. Further deterioration of the buried drums would allow a continued release of suspected hazardous components to the environment. IV. RESPONSE INFORMATION A. Situation l.Removal Actions to date On January 16, 1997 the OSC mobilized the ERCS contractor to remove and secure the suspected buried container at the site. Twenty-five of waste containers were exhumed. 137 drums were collected from the immediate area. Three containers of contaminated soil was placed in roll-off boxes for subsequent disposal. 2. Enforcement The operators of the Cristex facility were notified of there potential liability during the October and January activity. Mr. Marion Munn, a local representative, is the site contact. Mr. Munn gave permission to EPA to sample an above ground storage tank that displayed spillage similar to the material in the buried drums. A comparison of the analytical results indicates that the materials are the same. Records at the City of Oxford, City Engineer document the Cristex facility's clean-up of a #6 Diesel spill in 1993. 2 I I I I I I I I I I I I I I I I I I v. COST INFORMATION The following table details site expenditures associated with the Cristex Drum Site. ERCS ERCS ERCS Start Disposal Personnel Equipment Vendors Cost Co13t Actual $32,843.0 $4,401.43 $41,699.34* $5,370.19 $6,110.00 *Total includes the Waste Disposal Cost. VI. Disposition of the wastes Six bulk waste groups were disposed at Services of Florida in Tampa, Florida. the disposition of the waste. the City Environmental The table below outlines Wastestream Medium Quantity Contaminant Treatment Disposal migration Control CD-02 Organic 55 gallons Overpacked Non-HAZ Fisher Sludge Landfill Industrial Glencoe, AL CD-06 Organic 55 gallons Overpacked Non-P.AZ Fisher Sludge Landfill Industrial Glencoe, AL CD-07 Flammable 55 gallons Overpacked Fuel Fisher Organic Blending Industrial Liquid Glencoe, AL D001 CD-14 organic 55 gallons Overpacked Non-HAZ Fisher Sludge Landfill Industrial Glencoe, AL BG-01 Organic 935 gallons overpacked Non-HAZ Fisher Sludge Landfill Industrial Glencoe, AL BG-02 Flammable 55 gallons Overpacked Fuel Fisher Organic Blending Industrial Liquid Glencoe, AL D001 BG-03 Aqueous 165 gallons overpacked Non-HAZ Fisher Liquid Landfill Industrial Glencoe, AL 3 I I I I I I I I I I I I SENT BY:E RR B INTRODUCTION 1-6-87 4:08PM 918 733 4811:# 2/ 3 UNITED STATES ENVIRONMENTAL PROI'ECITON AGENCY REGION IV REMOVAL ACTION FACT SHEET Cristex Drum Site Oxford, Granville County, North Carolina n.cemb<r 1996 This fact sheet on the Cristex Drum Site has been prepared by the U.S. Environmental Protection Agency (EPA) to inform the public of the planned site removal activities. The Cristex Drum Site (the "Site") is an abandoned drum dump in north-west Oxford, North Carolina. The Site contains an unknown number of drums, buried and scattered throughout a one acre parccL Various drums of characteristic hazardou.~ waste, solvents, and adhesives have been positively identified by the site i11vestigations. The Site was unsecured upon EPA's arrival. Toe proximity of the Site to adjacent neighborhood significantly increased the chance of pedestrian intrusion and possible exposure to the substances within. After a review of the site conditions and analytical results confinning the past and possibly , ongoing releases to the environment, the OSC delennined an imminent and substantial release and treat of relca.se existed at the site. Immediate actions were deemed necessary to mitigate current !)roblems and eliminate future ones. EPA will sample the individual wastestreams and submit the samples to a laboratory for confirmation. The sample confirmation and identification process will take approximately three weeks. After the analytical results arc received by EPA, the plans for the ultimate disposal or treatment of the waste will be initiated. Total disposal of the w~testreams at the site depends on the disposal facility's acceptance of the waste. 1EPA has no control over any of the disposal facilities. While EPA is· preparing for the disposal of the waste, the on-site pel'lionncl will temporarily return to their home offices. This is done to reduce site cost. In the absence of any on-site activity, the site will be monitored by security serviees. I I I I I I I I I I I I SENT BY:E RR B ; I-6-97 4:10PM E FA REGION IV➔ 919 733 4811;#.3/ 3 \ EP A's proposed actions for the site can be divided into two basic areas: Contaminated Soil I. Identify the areal and vertical e,ctent of soil and sediment contamination. 2. Excavate and secure soils identified in the contamination SUIVey. 3. Sample all wastestreams to determine the disposal requirements. 4. Treat aod/or dispose of the identified contaminated media. Drummed Material 1. Consolidate and stage all containerized material. 2. Sample all wastestreams to determine the appropriate disposal profilc(s). 3. Treat and/ur dispose of the identified contaminated media. Based on .the information nvailable at this time, tho proposed removal activity will abate the immediate threats identified at the site. If funher remedial actions are necessary due to the presence of groundwater or other contamination, then the proposed action will remove the primary sources of groundwater contamination and aid in the long tcnn clean•up goals. An Administrative Record File, containing general site information, will be transported ll.lld stored in a local library .. Details on the exact location will be provided once arrangements have been completed. For additional Information, plense c~ntact the following EPA representatives: . . I (Technical and Specific lnformat,on) Mr. De'Lyntoneu• Moore On-Secne Coordinator U.S. Environmental Prntection Agency Emergency Response and Removal Branch I 00 Alabama Street, SW Atlllllta, Georgia 30303 (404) 562-8756 {General Information) Mr. Michael Henderson CommunitY Relations Coordinator U.S. Environmental Protection Agency Emergency Response and Removal Branch · 100 Alabama Street, SW Atlanta, Georgia 30303 ( 404) 562-8724 I I I I I I I I I I I I MAR-24-97 MON i2:09 OHM COF.P ERCS GOVT SERVS FAX NO. 4047297200 March 21, 199i Tony Moore USEP A Region IV 100 Alabama Strett Atlanta, Georgia 30303 .# OH:\,! Remediation ~ Sen·ice, Corp. "'-====-.4. IIIHUt:ai,· Ill Qte( ~\;on Re: MobiliZJition of Cristex Site. USEPA Delivery Order 4003-F4-060 OHM Project 19422 Dear Mr. r-.foore: P. 02 OID.1 Remediation Services Corp. (OHM) appreciates the opportunity to serve your remediation needs. OHM has tentatively scheduled the final phase of work for the Cristex site to begin on Wednesday, March 26, 1997. OHM anticipates the work will take three days to complete, inclucing c:obilization and demobilization. I have attacr.ed a:, estimated schedule for your review, The following is a brief description of the scope of work: MobiliZJiticn OHM wii! mobilize crews from our Covington, Georgia operations center. A rental track loader with a four way bucket will be delivered to the site by r.oon on March 26". Scope of Work Beginning the afternoon of March 26°, OHM will replace and re-grade staged soil stoclq,iles into previously excavated pits. The soil is RCRA non-hazardous and will not be shipped for off site disposal. lt is anticipated that the re-grading effort will be completed on Thwsday, March 27". Upon c.omp)etion of the re-grading activities, the newly contoured area mll receive an appropriate portion of grass ,.,.d and will be lightly covered v.ith straw to prevent erosion. Upon completion of the seeding aethities, OHM wii! prepare all rol!off containers and drummed material for disposal. Disposal subconrractors have been scheduled to a."Iive on site early Friday morn:ng. Upon shipment of the rolloff containers and drummed waste, OHM will demobilize ~ site. • E fl D E E I I I ~AR-2,-97 MON !2:10 OHM CORP ERGS GOVT SERVS FAX NO. 4047297200 F.03 Due to the short time frame of the project and "'th OSC approval, OHM recommends that cost capturing activities be performed from the Norcross home office. RCMS 1900's will be ~abmined to the OSC by March 28, 1997. Demobilization After completion of the above described tasks, OHM will demobilize personnel and equipment from the sire. The following is an estimared l:s: of personnel and equipment necessai,• to perform the ac1ivities described above: PERSONNEL Response Manager (I) Equipment Op=..tor (I) Recovery Technician (I) EQUIPMENT Pickup Trucks (2) Track Loader w!4 way bucket Sr.lBCONTRACTORS MKC Enterprises, Inc. Wil Transportation BF! U. Yates (Covington, Georgia) TBD (Covington, Georgia) TB_D (Covington, Georgia) Co,ingtcn Rental/Hertz/NC Drum Disposal T rar.sportation of Rolloffs Disposal ofnon-hazordous soils from rolloffs i'lolt!.S: U. Yain ls c1'rrerttly .:ma project in NC 1tnd wUI mobiUufrom thaJ siJL Additionally, the current delivery order expired on Febr.iary 16, 1997, and a delivery order extenSioo is needed prior to mobilization. The c1.1mnt ~ite ceiling ofSl00,000 is 84% expended. Should you have any questioIO.S, please do· not hesitate to call me at 770-453-7642, or page me at 800-999-6710 pin 11997601 &. Sinccn:ly; (1o-: ~7:J:0 . om~MEDIATION SERVICES CORP. Rand Bez:.efield U -- Project :.1anager cc: Randy Bennett (Operations Mgr) U. Yates (Response Mgr) File 19482 == == == == == == == == == == ---------~-------- OHM REMEDIATION SERVICES CORP. Cristex Drum Site tylll[! Mobtllz.alion 1.f!a--St~ Soil 0.,ding : ,:,a __ ., Seedlng/Erosioci Control ,_ ____ .,waste Preparatl~ for Shlppment l..f/f1 Wa&te Shippment · · ·t911 Sito D8mctifl.liii100 -----------t--- liiiiiil C, ---···--·-·····----- IJl!ilRCMS 1900's ~bmillal -------------------- ------------------ __J D I I I I I I I I I I I I I ,, NON-HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFESl I If waste is asbestos waste, col'nPlete Sections I, II, III and IV. If waste is MQI asbestos waste; complete only Sections I. II and III. No. 016557 Section I. , GENERATOR (GeneratQr~plete,-all of Section I. BFI WASTE CODE J. Description of Waste: · f ,., c.\ GENERATOR'S CERTIFICATION: I hereby cenify that the aOOVe named malarial is not a hazardous waste as defined by 40 CFR Part 261 or iiny applicable state law, has been properly described, classified al'\d packaged, and Is in proper condition for transportation according to applicable regulations: AND, It the waste I• a treatment residue ol a previously restricted hazardous waste subject to the Land Disposal Restrictions. I certify and warrant that the was1e has been treated in accordance with the requirements of 40 CFR Pan 268 and is no longer a hazardous waste as defined b( ~O CFR Pa~ 261. .-f , (,. l-·f;-.j":'"(:',.1,.:-t!, t.l.~-·-1·=1 •. {'·•,\';-: itr.,..L., ,:{, .. :-j, Generator Authorized Agent Name _:.:c.._~...:..:...:..c.~---- S i gnat u I e Shipment Date a. Name: . \ TAAN$f_QATEA I -. , TRANSPORTER II \J _) 1 I ,.__ \ r· · r V-, c-c ~ · _.. · · \ .. , ,.__ ~ ~-h. Name: p y M' Y' 0 = POUNDS YARDS CUBIC METERS CUBIC YARDS OTHER -~-~·LP'~+-7 ::~;-~,.\o\=--i--~~ci:..2.Q b. Address: __ _::;:;..._: ___ _c.:..__-=.J __ _:S-_;::..c....;::::::::,~. 1_-J:. Address: ____________________ _ (' <)I L)r,,.~,_1::.,\Ci :~)c cJ.7·d c ~~ j. Driver Name /Title: __________________ _ "<_"5 /4 1.t rt I-} .. 1 -i ~ 1~ ,,., ,-.s ,,,,..111 Pd .. c. Driver Name /Tit!e:~-~=--------'----'------~-::" i'.)~ ;•i&::,• >-(•·,PRltf_!_TYPE 17:;;:.l ") PRINT /TYPE d. Phone No.: / _..,'~•Truck No.:-'--'--''--'--'---k. Phone No.: ____________ I. Truck No.: ______ _ H-2 . -,r,-. . -I. Vehicle License No./ State:_, _, __ c/c/c··-··_:x_,._-___ ,_ •. _•; __ cl_, ____ _ m. Vehicle License No./ State: ________________ _ Acknowledgement of Receipt of Materials. Acknowledgement of Receipt of Materials. ~·· \'' -··, -(· ,,.., \. ~;;f•:L,~jtL--~..J.'/..'A..,, . .,,_, /.).J,;l,.1,..-t-- g. o,,._s, nn Shipmen! Oal■ o. ------------------Qm,er Sionsiure I I I I I I Sh,pment Data Section m -0 ESTI NATION cGeoerator comptete. e-d, oostination aite comptetes e-t.J e. Discrepancy Indication Space:--------------------------------------------- 1 hereby certify tha! the above named material has been accepted and to the best of my knowledge the foregoing is true and accurate. I. ------------N•m• ol Authorlzed Alil"\1 I I I I I I I R«eip10a!e Section IV ASBESTOS (Geiierator complete a-d, I, g'. OptlratOI' • ~plates e.) a. Operator's• Name: ___________________ _ b. Operator's• Phone No.: _________________ _ c. Operator's· Address:-------------------------------------------- d. Special Handling Instructions and additional information: OPERATOR'S CERTIFICATION: I hereby declare that the contents ot this consignment are fully and accura!ely described above by proper shipping name and are classl!,ad, pack&( marked, ar.d ta.baled, and are in all respects in proper condition for transport by highway according to applicable international and government regulations. e. Operator's Name & Title: ____________________ _ Pnnl/Type I. Name and Address I I I I I I Cate <· of Responsible Agency:-------'-------------------------------------- 9. D Friable; D Non-friable: □Both ____ _ % lrieble _____ _ % nonfriable C)ptlrator refers to the company which owns, leases, operates, controls. or supervises the !acility being demolished or renovated, or the demolition or renovation operation, or both. L· --... ----··---· ----· ---· -· GENERATOR AFTAIN .. --.. -----. 0231-720BMl D fl I .,. I I I I I I I I I I I I I I I -,,,,z..sa ,, .•• , A WILLS COMPANY .IOl~ll ( ~ ·-, "" Al. f\ = CUS10,,,fR .ioi.J ,v\ ~- ,,-1' STATE <' Wills Trucking 3185 Columbia Rd. Aichlield, Ohio 44286 In Ohio 800-362-3570 02324 WTI# ____ _ CIF# Outside Ohio• 800-321-3197 <-2 2'-9 7 O,.TE: DUl...,.TIOOI s:.,,. . r ,, --l~ • on -I -., r(''"" V .,.- MANIFEST , • c, 1 r . ~s-1 PO/OR# IOIU)()()(J(J(k)t)l)(J; EQUIPMENT# REVENUE PAY WEIGHTS- TRUCK '-1' -'] HEAVY- TRAILER c,,:;:s LIGHT - SET DROP , • • • ,,•.f!11i11:11l:i(;·'·S*'~ ..-, ,-~-..si-,.:jl~;,5 ~~--:'K".'.'V:-0 M~~~~t,. .:'!..' .,:,;,fi•:.1' > ~U;.~ ~~./1-;•~J. ,t,,<f'1t,,•_.,_~;(\· PULL 2 C, 22 ·.~ ~~_a,,~;~if;~~,t?\?-~i:) ~.ff!::' •. · .-.. -! }' •::_~1-l0· UNER l<OURLY -· DETENTION TIME TOTAL HRS. FREE BILL RATE TOTAL TIME JOB SITE s, .... , .. ~ DESTINATION SIAl'IT "~ OUT IN FRONT REAR FRONT REAR LEFT SIDE Q □ LEFT SIDE Q □ I I I TOP TOP I CHAINS I I CHAINS BINDER BINDER RIGHT SIDE TARP RIGHT SIDE TARP I CRANK I I CRANK BOWS BOWS FLOOR FLOOR PUU. ROPE PUU.ROPE ~ I ~ EQUIPMENT CONDITION (Remarks) EQUIPMENT CONDmON (Remarks) DRr.'ER~ SIGNATURE .S.(},._,..1,;_, ~ u.z.u..£) V ' :/.// CUSTOMER'S S!GNATURE-o-!"-_/-,-t{A,._/"S_•L-l .. '!'_, ~-c.•,,._, ______ _ '/ 0 D n D E D I I I I I I I I I I ,, NON-HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFES1 If waste is asbestos waste, complete Sections I, 11, III and IV. 1f waste is NQI asbestos waste, complete only Sections I, II and Ill. No. 016558 Section I. GENERATOR (Genarii10r CQmplE1!8!1 al\ of Section I. a. Generator Name: ----""-'-lc..,,'-[=·.J·lc.:'.ci.,_\_---'-j _,.~_·_. '-' :.ci (c_.-,._, ~\Ll,.1 ___ _ b. Generating location: c. Address: 11 /11 •r i (, i ,··· .-::;\.r,-•j ~.:,.\~). d. Address: i V· li'''i.lu /1\ i,-. .. :/ /\ ==•./. -::•,r-. :;; ·, e 'I I I ,, I .'., --;, -1 " ( . e. Phone No.: J ;·L ~-., ~ · •--' c, I. Phone No.: ()y i·J ( If owner of the generating lacillty differs from the generator, provide: g. Owner's Name: ~),_J_'--c.• _,,["';' =!'·='=·•:::;''-;•' •=''::·~1::ir=•=· ::' -;-\ \;:,':::/;:[=. ·=··='::;:f:::•;:::=:;::...C:h. Owner's Phone No.: LI r l.l t.:; /,. 'Cl •~ {, i. BFI WASTE CODE ~ fillklh k bbbl 11 IJlsbl1 l?ilJ Containers j. Description of Waste: 'oil '·1:r:i,1 I 1-~ ~ffi -~-""' '~''_,_)"'0 .. · ·.._i 1.__<.,_;r.,_,w; )'--'--_J"' .. .,_n-"l-· ______ · · -· · · l!J t1'.J L!J_J GENERATOR'S CERTIFICATION: I nereby certify that the above named material is not a hazardous waste as defined by 40 CFR Part 261 or any applicable state law, has been property described, classified and packaged, and Is in prope1 condition for transportation according to applicable regulations; AND, II the waste 11 a treatment .... ldue of ■ pr■vloualy ..,..trlcted hazardous waste subject to the Lal'ld Disposal Restrfetions, I oort,!y and warrant that the waste has been treated in accordance with the requirements of 40 CFR Part 268 and is no longer a hazardous was111 as defined by 40 CFR Part 261. '· I ,, •-• Generator Authorized Agent Name Section ll TRANSPORTER I TRANSPORTER 11 = OM -MET AL ORUM DP -PLASTIC DAUM B -BAG BA - 6 MIL. PLASTIC BAG or WRAP T TRUCK 0 OTHER !.lliilli P POUNDS Y YARDS Ml CUBIC METERS yl CUBIC YARDS 0 OTHER V, I: i I; 1· , , ," /,-" , a. Name: --1_.!.!..!.LL.:'-Ll.c..!..'..L...!C...!_ 0 -'--''-. -'-J---------h. Name: _______________________ _ b. Address: _'__sl::..-_' L(J./_-"--"-->-'-'-'''-'''-'"-:.-''~L-------.·. i :' 11 Ii; '·:1 ,.,·. I{/ i. Address: ______________________ _ c. OriverName/Title:·\· :-r, (~ .. 1,J ,.,,·" /1 f-f (,.-,l) ,··, ·~ I ' I PRINT I r.lPE -· -; d. Phone No.:'/ (,. ?, f I ··-1..-J • ·\ /., e. Truck No.: f · f .__ j. Driver Name/Title: __________________ _ PAINT /TYPE k. Phone No.: ____________ I. Truck No.: _____ _ I. Vehicle License No./ State: ..,_i'•~'S: .... Lf_· ,J.:;_'L/.:.'~~---'''--:.:.1.:...-:.:.1·'-------m. Vehicle License No./ State: ________________ _ Acknowledgement of Rec~ipt of Materials. g. ,\( ,:f---1 i--G-1. '."_.,,CA >3)} ·(I-. 1 '! I Dnve, s, tura 1, le 1,·d; I;· I Sh,pmem Oa1e Acknowledgement of Receipt of Materials. I I I I I I Sh,pment Da1a Section Ill DESTINATION (Generstor completes s-d, 08stinstion site compleles &-1.) a. Site Name: --''·'"-'~'-'--...-~·.,_• c'c...,•_' c; ,-c•cl c' c' .:.' cl .:_d'---'-l-'-1-'-'"''-'-' si_\,._,;-'-J _./ __ c. Phone No.: (j I {) C: __ ~_; ,-:-, ~ ":J j :.;,) _:j_ b. Physical Address: _.,_/_· L_.f )_,"-\ '-· ,_/ _..,--~'-'--'C"-'-·',_{:.._\,_· .:."-''-("'J'---_,\_.j_,,v-"-'"t•I __ I r,Jc. d. MailingAddress: ·1·•.() •¥t,(.:y -~i()q(p )-'r:':·h•r1: Ni~ r:X.j'l~.L e. Discrepancy Indication Space:--------------------------------------------- 1 hereby certify that the above named material has been accepted and to the best of my knowledge the foregoing is true and accurate. ,. --------------I I I I I I I Signatur• Rac:;eipl Date Section rv· ASBESTOS <Genetator complete a-d.· tg. Operator· oomp1etas e.J a .. Operator's• Name: ___________________ _ b. Operator's• Phone No.: _________________ _ c. Operator's• Address:-------------------------------------------- d. Special Handling Instructions and additlonat information: OPERATOR'S CERTIFICATION: I hereby declare that the contents ol this consignment are fully end accuratety described above by proper shipping name and are class1!1ed, packe msrked, end labeled, and are in all respects in proper condition for transport by highway according to applicable international and government regulations. e. Operator's Name & Title:-~~-------------------- PM1/Typa t. Name and Address Operato(t • S>gnature I I I II I Date of Responsible Agency:-----------------------------------~----------- g. 0 Friable; 0 Non•lriable; 0 Both ____ _ % friable ____ _ % nonfriable Operator refers to the company which owns, lesses, opera1as, controls, or supervises the taci11ty being demolished or renovated, or the demolition or renovation operation, or both. · -· ----·-----. ··--·------·--_______________ GENERATOR RETAIN ..••. _ _____ ... _________ . __ -·--__ 023,.1200819 ti ff g g 0 0 D 0 D 0 D D 0 n 0 n I I I I 01234 Wills Trucking ,,.,a..sa . , .•• , 3185 Columbia Rd . Aichlield, Ohio 44286 In Ohio • 800-362-3570 WTI# ____ _ CIF# A WILLS COMPANY Outside Ohio• 800-321-3197 J / ,, ,-h I\ ,. O.UE: .oe ~1, e'.?;,----,__)'.;~ --}) -•->..w, ~~ 0£511,.All()H ..-•:f(,t,-.,-_ . ..__,.,f-,<-e,,_,] " -,_.,yv,.J·_ r.-: .. ,'-i.:2:::Y-P 0" 0 ,,.::--;,.-<.Ji --,1,el~U o .. /d-.. ~YJe,,.A,,Q , i//. -e,;.saTE ClJ510MtR 0 H /l-1 MANIFEST# -0 I 6 55'(.PO!OR# Xll.llXXXXXXXXXXX EQUIPMENT# REVENUE PAY WEIGHTS- TRUCK / 7 'L HEAVY- TRAILER (, 3 b LIGHT- SET DROP METER s·: .. .::,, i}t:~1"\ _E~,t,~'. . . (, I ob . ~,,.._, . ,,.. . PULL HUB .s'. ;..(\:f!:·i".J!'>.~\:-E ), .• -· .. ' . LINER ii~>~' ..;i,',.' -· I -· DETENTION TIME TOTAL HAS. FAE£ BILL RATE TOTAL TIME JOB SITE $TART .. ~ DESTINATION 51AAT .. ~ OUT IN FRONT REAR FRONT REAR LEFT SIDE Q □ LEFT SIDE Q □ I I I TOP TOP CHAINS CHAINS ' • I ~ I I I BINDER BINDER .. / . . / RIGHT SIDE . TARP/ RIGHT SIDE TARP '· I CRANK ', ' I I CRANK BOWS BOWS FLOOR FLOOR PULL ROPE PULL ROPE 3 I 3 EQUIPMENT CONDITION (Remarks) EQUIPMENT CONDITION (Ramarks) ~ /:·f(-:. 01rr,..,1 DRIVER'S SIGNATURE_:~:..· _--ft..•:..'~..:·•:5-,J.L'A='-"-1-":c··-''C.'·•-::'.;./_--~ef.::_-"i._l__:.-/c.A:..L ?' (/ CUSTOMER'S SIGNATURE ____________ _ B 11 g g g 0 0 D 0 D D D D D 0 D D . '. • ~ON-HAZARDOUS SP,~CIAL WASTE & ASBESTOS MANIFESl If waste is asbestos waste, complete Sections I, II, Ill and IV. NO. Q 165 5 9 If waste is .tfQI asbestos waste, complete only Sections I, II and III. Section L · '. GENERATOR'S CERTJFICAT16N: I hereby certIty that the above named material is not a hazardous waste as de1ined by 40 CFR Part 261 or any applicable state law, has been property described, classified and packaged, and Is in proper condition for transportation according to applicable regulations: AND, lf the w11t1 ls e treatment residue 011 previously restricted hazardous waste subject to Iha Land Disposal Restrictions, I certity and warrant that the waste has been treated in accordance with lhe requirements of 40 CFR Part 268 and is no longar a Generator Authorized Agent Name Shipmen! Date haza~ous wasta as defined br 4? CFR Part 261. _ lt L·\·;'·:.:·,-!<:.1.•. l\.'',.,:t,··1:'-1.: /, .. \<.',1 l, ,_',.,::(,) _.;,.•f-=s,,-oa"',,'-,.--'------~ Section II TRANSPORTER (0eneratorcomple18·a-d; fr:n5~~l1~18 E!'il,) p y M' Y' 0 Lu \ \ TRANSPORTER I ""T•-L)( __ \'-...,1 TRANSPORTER II .~. rv-I ' r a. Name: ~-·· ·, ~ h. Name: . ,.} (p '·.f 7 ~:i h-0~ ~'i ,--.... 0.~ c\( b. Address: i. Address: L I , \ c ... "·,(__ c;'--jJO~ (_)', u r-,-. i.-,. -~ r--. )( ( \ I (' ·.Jo1\1-r-S •, k~ C·< ~. c. Driver Name/ Tille: ,,, • ' . 'I' ... j. Driver Name/ Title: '1;.0·5 7 7( '1"1."''W"" r · · PAINT /TYPE ' 10 ' d. Phone No.: p __,J e. Truck No.: I(;. \i'-/ b k. Phone No.: L Truck No.: (: F 'i'j '.':-·' '! m. Vehicle License No. / State; f. Vehicle License No. / State: Acknowledgement of Receipt of Materials. Acknowledgem~nt of Receipt of Materials . . \ ... . ........ \ ,./ _..,..,,....· I , I-1, lb 11 Ii I I I I •· X_,; C.'1{,_,,,.,,. .!_ .. · ·, )4'---"· I I °""" S1ena1ur1 . .I Shipmen1 Date om,., Sl!lnature Shipment Date Section m 0 ESTI NATION (Generator completes a~. destlnatlon' .,;+e completes .u . . .. :5--, ... ,",<()1'..) Lou, ·-,~. --J L~,.:i .. r--,.-U t-·, i I '-/ /U -,::-,-. . -· 4 I 3 d... a. Sita Name: . l ' '\ \_.. ·-Phone No.: ..... ~~ C. --,· - I e. Discrepancy Indication Space:---------------------------------------------- 1 hereby certify that the above named material has been accepted and to the best of my knowledge the foregoing is true and accurate. !~ Name of Authorized Agen1 Signature I I I I I I I Rac11pt Date Section JV'; · ASBESTOS (GOOffl.torcompfete 8~.'1. g,'Operalor···complet8S e.) . a. Operator's· Name: ___________________ _ b. Operator's• Phone No.: _________________ _ c. Operator's• Address:-------------------------------------------- d. Special Handling Instructions and additional information: OPERATOR'S CERTIFICATION: I hereby declare that lhe contents of !his consignment are fully and aCCtJratety described aboVe by proper shipping name and ara ctass,t,ed, paeke marl<ed, and labeled, and are in all respects in proper condition for transpert by highway aceon::hng to applicable international and government regulations. e. Operator's Name & Tille:~~~--------------------Print I Type I. Name and Address Operator's· Signal~•• I I I I I I Date of Responsible Agency:----------------------------------------------- 9. D Friable; D Non-friable: D Both _____ _ % friable _____ _ % nonfriable Operator refers to the company which owns, taases, operates, controls, or supervises the !ac,hty being demolished or renovated, or the demol11ion or renovation operation, or both _/_._ ----·•-·· ~ENERATORAF-TAJN___ -·------0231-720BM I I I I I I g I I I I ,,.,a..sa . , •. , A WILLS COMPANY ~ ) = "" Ll 5 I::' f✓,'..J, 4-, ~ -IV "" 1<)y {-.'.,..,,{ ' "'~lt_.smE CU$10MEII , Wills Trucking 3185 Columbia Rd . Richfield, Ohio 44286 In Ohio • 800-362-3570 01612 WTI# ____ _ CIF# ____ _ Oulside Ohio· 800-321-3197 ""' Z-~·?7 . - 1om,,. .. rl()N .. x:,u,Jt;c)...(~1..,i•l. l~ Hr/·\, II ON -j;c-,, ·o J1. c.. ITATE MANIFEST#·()/{__ _', :,-PO/OR# XXXIIXJOO(l(l()()l){)( EQUIPMENT# REVENUE PAY WEIGHTS- TRUCK /l \' IIV( HEAVY- TRAILER (,,. <JI LIGHT - SET DROP ,., _ _,~ ,.~ ' ' . ,-•e· ··'"' . k 1/ I -,.!~.,,,,~ ... -~ ' u ,,,,:Jro.i...: . . . ' ~ "' .; PULL t"~ 'E~-}E_-LINER 11;,!i't ,.__ • ' ,;;;;Ji,:,,._ • '~ ,J'. .• • ' . MOUIILY -DETENTION TIME TOTAL HAS. FREE BILL RATE TOTAL TIME JOB SITE .,_ "~ DESTINATION STAAT •= OUT IN FRONT REAR FRONT REAR L£FTSIDE w □ L£FTSIDE w □ I I I .. TOP TOP I CHAINS I I CHAINS BINDER BINDER RIGHT SIDE TARP RIGHT SIDE TARP I CRANK I I CRANK BOWS BOWS FLOOR FLOOR PULL ROPE PULL ROPE 3 I 3 .· ' · -;Q;j~NT Cz;;(Reit -:),< ~ ,-'-'-' EQUIPMENT CONDmON (Remarks) D~· .----7 ' '! i /"' /';~ ,/ DRIVER'S SIGNATURE',--./ l_,\l/,~-CUSTOMER'S SIGNATURE I I I I I I I I I I I I I NON-HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFESl No. 016560 II waste is asbestos waste, co~Pi'ete Sections I, 11, III and IV. II waste is IBn: asbestos waste, complete only Sections I, 11 and 111. Section I.' GENERATOR (Genel"ator~pJetes an 01 Sact1on 1. a. Generator Name: l ) ~ r-? .l\ \<_ --e. :: '" i O A ) \ V b. Generating Location: _ _,C:.~.,.r~_··~'-~"Q~• -'\;,._··-~~···c..;_~_;' ::'s..' ___ _ 'nr, A\,:>..hcu-00.··--,._\-ree-L µ,,_,,, S,;; \;,,T~·-.-•Cu·.1.," c. Address: I L -. __ ,. l d. Address: ---'--'-'-6....:f---=-'-'--'""-'--'-· --"'-'--""""--'-'-- ::. ~ ~ i i 1' YA--Fl t . ...'o ~-A+-\ (\f\ \-o ·c;:_A ,.~\O ··:~ ~)'~S t·> r ; 1 vf. ::...1.r--)'~i-· ::::·,v~-?,7r:;~D /Jv ... ri1~.A./ t,J( e. Phone No.: -~...,~L----,-~~~-'--"--~--~~~-~--I. Phone No.: __ _:_,:_..:c~:.:..c.:.c...c..,_...__..,_..::,c..., _________ _ If owner of the generating facility differs from the generator, provide: E RRJ::; 11 o" __ ,-:-:_ 1 ,---.,~ --~-7,-:-: 1,,..., g. Owner's Name: ~~--'"';:::::;:::-:::;';:'::;=:;::::;'';::::;::::::-;'::.-/;.=;::::::;:cc"· 0w-:::,~oe~'c'c,':P~ho~,~•~N~o::·'.:;::"-t:::::;=-7_,__~'-'-V.=-=~---'LC._,','.v/;' ,;!e•-"--- 1 N lc 11121: bl'---'-'--'--=--½-"-'--' bJ:,bl I b IG:.I Coota;oe,s g~: ~c::~~~M i. BFl WASTE CODE r-.... 8-BAG ::. (') .\ \ \_.)·(: \·"'°' r ; ~ :J() ·., k. Ouanti, Unrts No. TYPE BA • 6 MIL. PLASTIC BAG j. DescriptionofWaste:,_,=7 ~~~=--'~~-~'c,~='-'--'--'--r.::J c::T:7 ~ orWAAP ;,.,'.'.I oi·i":i;:'-":.,r,•,\'\ ., l,'1° 11111!1 e.Ji.JW;; :;;~~~~ GENER_A_T_O_R __ S_C_E_R_T_<_F<_C_A_T-,O-N-,-,-"'-"_b_y_~-,-,fy-<h,-,-~-.----.-ra-m,d----,.-"'-,-"-not a hazardous waste as dellned by 40 CFR Part 261 or J.!.tl.lI.S. any applic:able state law, has been properly descnbed, class1lied and packaged, and is in proper condition for transportation according lo P POUNDS applicable regulations; ANO, II the w11te 11 a treatment rnldue of I pravlously restricted haurdous waste aubj&Ct to the Land Disposal Y YARDS Restrictions, I cert1ly and warrant that lt1e waste has been treated in accordance w11t1 the requirements ot 40 CFR Pan 268 and is no longer a M3 CUBIC METERS hazardous waste as delined_by40 CFR Part 261. Y3 CUBIC YARDS ii·c-r,r•·,!,..·i·:.i\.,l,'.--·pr •1-i~·'. .. /, ,,_. .i ·-M~ .. -· 1(:1_;,121·::1,-1·11 ~ _0~:~;:s Generator Authorized Agent Name Signature Shipment Date Section II TRANSPORTER {Generator complete a-d; +~~rter I compl':-~n \ TRANSPORTER I TRANSPORTER 11 '' ) I 1\ ~. Tr-uc \'\ -: -~~ a. Name; \e 3 , h. Name: ,~ ,,., q:z .-~· ~-~r. ~::, ;.....:.r-.c,. _,...~) b. Address: ....., = ;. Address: (~ l'"'l!l -..,;~c, \ -~ ; 1•j :,c ,··, ,.. ,.., ,-) c-:.i c,~/) "· :i Driver Name/ Title:\"(.-/1 t I'<;.-: ../ f"ltl'!t._L "'·!I C. i j. Driver Name/ Tille: Phone No.: 1.,"r)3 PR!ITTITYPE i >j_ PRINT /TYPE d. 77(e Y73<n e. Truck No.: .. k. Phone No.: 1. Truck No.: ··.-.,µ 7,·, -, ,. Vehicle license No. I State: I ,,. -m. Vehicle license No, / State: Acknowledgement of Receipt of Materials. Acknowledgement of Receipt of Materials. ' I. ,., J "{ k, I I, I" 11 171 I I I I I I g. \•q f·} "(i/'1.,-(,,1y?J._J/t~-...At..:: "· Dnv., s.,nature ,'/ Sf'lipment0...19 Driver Sinnature S~, men1 Date Section Ill DESTINATION <Generator completes a-d, destination ,tte comp1e1a1 e-1.1 e. Discrepancy Indication Space:--------------------------------------------- 1 hereby certify that the above named material has been accepted and to the best of my knowledge the foregoing is true and accurate. '· ~~~-~-------Nem, ol Authon.zed Agent s,g,,.ture I I I I I I I R-~Oa1e Section IV a. Operator's· Name: __________________ _ b. Operator's• Phone No.: ________________ _ c. Operator's· Address:------------------------------------------------ d. Special Handling Instructions and additional information: OPERATOR"S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accura!ely"tlescribed above by proper shipping name and are classi!led, packec mar1<.ed, and labeled, and are in all respects in proper cond11ion !or transport by highway according lo applicable in!emational and government regulations. e. Operator's Name & Title: ,,cMc,s,.c,,.=---------------------()pe<a!Or't' Signature I I I I I I Date f. Name and Address of Responsible Agency:------------------------------------------- 9. D Friable;· D Non-friable: D Both _____ _ % friab!e _____ _ % nonfriable Opera1or refers to the company which owns, leases, opere1es. controls, or supervises the facility being demolished or renovated, or the demolition or renovation opera1ion. or both. ---· ---GENERATOR RETAIN. 0231-1201'' I I I I I I I I I I .. ,,.,a..sa •..•• , A WILLS COMPANY JO~ WE / ,, i "' t-"' )(' "" f},c f ~vr, CUSTO ... E~ () u A ..... ' c:,, f e, SUlE 1 Wills Trucking 3185 Columbia Ad . Richfield, Ohio 44286~ In Ohio · 800-362-3570 .• l Outside Ohio· 800-321:3197 DATE 0HTINATl()N C..._,-,i •• 44610 WTI # ____ _ CIF# -Z,-,a....q"-] r_~ ... -f{, I -,,,, }· ,I/( CITY 1-?n~ '~Yr STATJ' Al/ - ''MANIFEST # -rn c7. ") PO/OR# :W:XlOIXIOOClXXXXX EQUIPMENT# REVENUE PAY WEIGHTS - TRUCK I O '-I HEA~~ TRAILER {:_( 'I-LIGHT SET ; .. DROP METER S '· E PULL 7 /"7 HUBS E LINER HOURLY I •OO• DETENTION TIME TOTAL HRS. FREE BILL RATE TOTAL TIME JOB S!TE START "~ DESTINATION START "~ OUT IN FRONT REAR FRONT REAR LEFf SIDE CJ D LEFf SIDE CJ D I I I TOP TOP I CHAINS I I CHAINS BINDER BINDER RIGHT SIDE TARP RIGHT SIDE TARP I CRANK I I CRANK BOWS BOWS FLOOR FLOOR PULL ROPE PULL ROPE ~ I ~ EQUIPMENT CONDITION (Remarks) EQUIPMENT CONDITION (Remarks) DRIVER'S SIGNATURE pj:~;_.;,;e~- g n D D n D D D u D D n n MKC Enterprises, Inc. This document will serve as the Certificate of Disposal for the material received at our Doraville Facility as indicated below: GENERATOR: MANIFEST DOCUMENT NUMBER: GENERA TOR CERTIFICATION DA TE: DA TE ISSUED: U.S EPNWWD/ERRB -Cristex Site I 00 Alabama Street, SW, 11th Floor Atlanta, GJ\ 30303 93717 03/27/97 04/08/97 This material will be properly disposed of in accordance with all required and applicable regulations, laws, pem1its and licenses. MKC ENTERPRISES, INC. ,S::l/1 -hU:~-: !. 1'"Vi'ce President -Administration EPA/EPD PART B PERMIT NO, HW-005 (S&T) GAD000616367 5856 New Peachtre Doraville. GA 30340 I I I I I I I I I I I I I I I MKC ENTERPRISES, INC. LAND DISPOSAL RESTRICTION FORM SECTION I. GENERAL INFORMATION ::, SECTION II. APPLICABILITY A. This shipment contains material for which the Land Disposal Restrictions (LDR- 40 CF.R 268) do not apply because: 1. _/_ They are not EPA regulated materials. 2. __ They are EPA regulated materials which may be land disposed without further treatment. List EPA codes: 3. __ They are EPA regulated materials subject to an extension to the effective date. EPA CodefTreatability Group (NWN or WN) Extension Date B. The Land Disposal Restrictions apply to these materials because they are subject to: 1. __ Alternate Debris Treatment Notification This waste is a debris and is subject to the alternate treatment standards of 40CFR268.45. The waste contains the following contaminants subject to treatment (check all that apply): 2 a. __ 268.45(b)(1) -Toxicity characteristic debris b. __ 268.45(b)(2) -Debris contaminated with listed waste c. __ 268.45(b)(3) -Cyanide reactive debris California List Waste CALIFORNIA LIST CONSTITUENTS 40 CFR 268.32 and RCRA Section 3004(0) _Cyanides _Nickel _Thallium _Liquid with PCB's . _Materials containing Halogenated Organic Carbon I I I I I I I I I I I I I I I I I I I 3. __ Solvent Wastes The following materials must be treated to meet the LDR standards expressed in the "Treatment Standards for Hazardous Waste" table in 40CFR 268.40 EPA Code(s) __ F001 _F002 __ F003 __ F004 __ FOOS F001-F005 Spent Solvents __ Acetone __ Benzene __ n-Butyl Alcohol __ Carbon Disulfide __ Carbon Tetrachloride __ Chlorobenzene __ a-Cresci __ m-Cresol __ p-Cresol __ Cresci -mixed isomers __ Carbon Disulfide • __ 2-Nitropropane •• WN __ Cyclohexanone __ o-Dichlorobenzene __ Ethyl Acetate __ Ethylbenzene __ Ethyl Ether __ lsobutyl alcohol __ Methanol __ Methylene Chloride __ Methyl Ethyl Ketone __ Methyl lsobutyl Ketone __ Cyclohexanone __ 2-Ethoxyethanol •• NWN __ Ntrobenzene __ Pyridine __ Tetrachloroethylene __ Toluene __ 1, 1, 1,-Trichloroethane __ 1, 1,2-Trichloroethane __ 1, 1,2-Trichloro-1,2,2-trifiuoroethane __ Trichloroethylene __ Trichloromonofluoromethane __ Xylenes -mixed isomers __ Methanol • * If these constituents are present alone or in any combination of the three, the nonwastewater forms of these constituents must ·be treated to TCLP levels as indicated in 40CFR 268.40. •· If either but not both of these two constituents are the only listed F001-F005 solvents, then they must be treated by the Technology- Based standards as indicated in 40CFR 268.40. 4._LRestricted materials subject to the LDR standards set forth in 40 CFR 268.40. For each EPA Code, list the constituent and/or subcategory, if applicable, and indicate with a check whether the material is a wastewater or a nonwastewater. Code ;Qoo I .PCTP2 Constituent/Subcategory WW NWW 1· SECTION Ill UNDERLYING HAZARDOUS CONSTITUENTS This shipment {)contains~ does not contain waste(s) designated with USEPA Hazardous Waste Code D001 -D002 and 0012 -D043 which contain underlying hazardous co~ tuents. For characteristic wastes, 0001-0002 and D012 -D043 that are subject to trearment standards in Table 268.40, ''Treatment Standards for Hazardous I Wastes," all underlying hazardous constituents must meet Universal Treatment Standards, found in CFR40 268.48, Table UTS, prior to land disposal. Table UTS --Universal Treatment Standards E {Check each constituent known to be in the waste(s} referenced above} -NWN -NWN -NWN (mg/l) (mg/Kg) (mg/L) (mg/Kg} (mglL) (mg/Kg) [I Acenapthy~ne 0059 34 [] 1,2-0ichloroethar,e 021 60 II N,trobenzel"lfl 0066 \4 (1 Acenaphthene 0 059 3• !] 1, 1-0ichloroetnylene 0.025 60 II 5-Nitro-o-toluid,ne 0.32 26 m 1] Acetone 0 26 ''° I) trans-1,2-Dichloroetnylene 0.054 30 II 0-N1tropnenot 0 028 13 [1 Acetonnnle 56 , 6 I) 2.4-DiCl'llorophenol 0 044 ,. II p-Nttropnenol 0,, 29 I) Acetopnenone 0 010 9.7 [l 2,6-D1Cl'lloropnenol 0 044 ,. 11 N-NItrosod,ethylamIne 0.40 26 [] 2-Acetylaminofluorene 0 059 1'0 II 1,2-0iCl'lloropropane 0.85 16 I) N-N1trosod1metnylam,ne 0.40 NA2.3 II Acrole1n 0 29 NA II cis-1.3-DiCl'lloropropene 0036 16 II N-N1troso-<:1i-n-butylam,ne 0 ,o 17 m II Acrylamioe 19 " {l trans-1,3-0iCl'lloropropene 0 036 16 I) N-N,trosometnyletnylam,ne 0 ,o 2.3 II Acrylonrtrile 0" 64 [l Dieldnn 0017 0 13 I] N-N11rosomoronol1ne o,o 2.3 I) Aldrin 0 021 0.066 ll Diethyl phthalate 0 20 26 II N-Nitrosop1pend1ne 0013 35 II 4-Am1nob1onenyl 0.13 NA 11 2,4-Dimelr"lyl phenol 0.036 ,. II N-N nrosopyrro!idine 0 013 35 II Aniline 0.81 ,. II 01methyl pnmalate 0.047 26 II Paratn,on 0 014 46 [I Antr"lrace_ne 0.059 34 !] Oi-n-buty! phthatate 0057 26 II Total PCBs {sum of all PCB 010 10 m isomers, or all Aroc!ors) 11 Aram1te 0.36 NA I) 1,4-Dinitroben.zene 0.32 23 [l PentaCl'llorooenzena 0 055 10 II alpha-BHC 0 00014 0.066 I) 4,6-Dinrtro-o-eresol 026 160 [l PeCDDs {All Pentachlord1benzo-p-0.000063 0 001 dioxins) !] beta-BHC 000014 0.066 II 2,4-Dimtrophenol 0.12 160 [I PeCDFs (all PentacnlorodIbenzo-0 000035 0 001 furans) I I) delta-BHC 0.023 0.066 {I 2,4-Dinitrotoluena 0 32 1'0 II Pentachloroetnane 0.055 eo I] pamma-BHC 00017 0.066 {l 2.6-0in1trotoluene 0.55 26 II Pentad'lloron1trooenzene 0.055 4.6 fl Benzene 0.14 10 IJ D1-n-octyl phthalate 0017 26 II Pentachlorophenol 0 089 7A I) Benz(a)anthracene 0 059 " 11 p-D1meIhylaminoa:obenzene 0.13 NA l] PMnacet,n 0.081 16 I) Banzai cnlonde 0.055 60 11 Di-n-propylnttrosoamine 0.40 ,. [J Pnenantnrene 0.059 56 I I) Benzo(b)-lluoranthene 0.11 6.6 [l 1,4-Dioxane NA 170 I) Phenol 0.039 62 I) Benzo{k)-lloranthena 0.11 6.6 [l Diphenylamine (d1thcun to d1slin-0.92 13 II Pr-1ora1e 0.021 ,.6 guIsh lrom d1phenylnrtrosoamine) II Benzo( g,h, i)-peryIene 0.0055 1 6 II D1pheny!nitrosoamine (diff,cult to 0.92 13 II Phthahc acid 0.055 26 d,stingu1sh from diphenylamine) II Benzo(e)pyrene 0 061 34 II 1 .2-Diphenylhydrazine 0087 NA II Phthalic anhydride 0.055 26 I II Bromodichloromethane 0 35 15 II Disu!foton 0,017 6.2 II Pronamida 0.093 15 II Methyl bromide (Bromomethane) 0.11 15 II Endosu!fan 1 0 023 0066 II Pyrene 0.067 62 U 4-Bromophenyl phenyl ether 0.055 15 II Endosu!fan II 0029 0.13 II Pyridine 0.014 16 ll n-Buty! BICOhOI 5.6 2.6 II Enoosullan su!fate 0.029 0.13 II Safrole 0.081 22 1J 81J1yl benzyl phtnalate 0.017 26 II Enorin 0.0028 0.13 {I Silvex (2.4,5-TP) 0.72 7.9 I I) 2-se::-Butyl--4,6-dinnrophenol (Dinoseb) 0.066 2.5 II Endrin aldehyde 0025 0.13 11 2,4,5-T 12.4,5-0.72 7.9 Tnchloropneno~yacetic acid) II Carbon d1sutfide 36 4.8mgfl 1J Ethyl acetate 03< 33 11 1,2,4,5-Tetrachloroben.zene 0 055 ,. TCLP II Carbon 1etrachloride 0057 6.0 II Ethyl benzene 0 057 10 (I 'rCDDs (All Tetraehlorodibenzo-0.000063 0.001 furans) I· [] Chloroane (alpha and gamma isomers) 0.0033 0.26 !] Ethyl cyanide 0.24 360 [] TCDFs (All Tetrachlorod1benzo-p-0.000063 0 001 dioxins) I] p-Chloroaniline 046 16 I] Ethyl ether 0.12 160 II 1,1,1,2-Tetrachloroethane 0 057 6.0 II Chlorobenzene 0 057 60 I) bis(2•Ethylhexyl) phtnalate 0 26 26 II 1,1,2,2-Tetrachloroetnane 0.057 6.0 II Chlorobe:,zilate 0.10 NA II Etnyl melr"laetyla1e 0.14 160 (] Tetrachloroetnylene 0.056 60 {] 2-Chloro-1.3-b\JliO.ene 0.057 0.28 I) Ethylene O~ioe 012 NA {] 2.3.4.6-TetraCl'llorophenol 0.030 7.4 I I) Chlorod1oromometnane 0057 15 II Famphur 0.017 15 [J Toluene 0.080 10 I) Chloroetr-1ane 0.27 6.0 fl Fluoranthene 0.068 3.4 II Toxaphene 0.0095 2.6 II bis(2-Chloroet!1Uxy} metnane 0.036 7 2 [J Fluorane 0.059 34 (I Bromolorm (Tribromometnane) 0.63 15 [I bis(2-Cnloroetn:,-I} ether 0 033 6.0 11 Hep!achlor 0.00,2 0.066 ll 1,2,4-Trichloroben.zene 0.055 19 {] Chlorolorm 0 046 6.0 [J Heptachlor epoxide 0.016 0.066 [J 1,1,1-TriCl'lloroetnane 0.054 6.0 I 1J bis(2-Chloroisooropyl) ether 0.055 7.2 II Hexachloroben.zel'\8 0.055 10 I) 1, 1 ,2-Tnchloroethane 0 054 6.0 l) p-Chloro-m-eresol 0018 ,. II Hexachlorobutad1ene 0.055 5.6 II Triehloroethylene 0 054 6.0 I) 2-Chloroethyl v,nyl ether 0.062 NA II Hexachlorocyclopentadiene 0 057 24 [] Trichloromonofluoromethane 0.020 30 I) Chloromethane (Methyl Chloride) 0.19 30 {] Hexathlorod1oen.zo-p-chox1ns 0 000063 0001 II 2,4,5-Trichlorophenol 0.18 1., (I 2-Chloronaph!halene 0.055 5.6 I) Hexsaehlorod1benzo-h.rrans 0.000063 0,001 fl 2.4.6-Tr1chloropheno! 0.035 7.4 IJ 2-Chloroohenol 0.044 5.7 [] He•ad'lloroethane 0.055 30 I] 1,2,3-Trichloroproparle 085 30 I I) 3-Chloroprcpylene 0036 30 11 Hexach!oroprope:-lft 0.035 30 IJ 1, 1.::-Triehioro-1.2.2Trrf!uoroethane 0.057 30 I} Chrysene 0.059 3.4 [I tndeno(1,2,3-c,d}pyte1"18 0.0055 3.0 ti Tris(2.3-d1bromopropyl) 0.11 0.10 phOsphate I) o-eresol 0.11 5.6 [l looomethane 0.19 65 II Vinyl chloride 0.27 60 II m-Cresol (d1ff1cult to d,stinguish from 0.77 5.6 !) lsobutyl alcohol {isob\Jlano1) 5.6 170 [) Xylenes-mixed isomers (sum of o•. 0.32 30 p-cresol) m-.& p-xylene concentrations) I II p-Cresol (d1ff1cult to distinguish from 0.77 56 II lsodrin 0.021 0 066 II Antimony ,., 2.1 mgfl TCLP m-cresol) II Cy~lohexanone 0 36 0.75m;II II lsosalrole 0081 2.6 I) Arsenic 1.4 5.0 mg/I TCLP TCLP II 1,2-0ibromo-3-chloropropane 0.028 15 II Kepone 0.0011 0.13 [J Barium 1.2 7.6 mgll TCLP I II Ethylene d10romide ( 1,2-0.028 15 (] Methacrylonitrile 0.24 64 (I Beryllium 0.82 0.014 mg/l TCLP Dioromoethane) 0 Dibfomoethane 0.72 15 1J Methanol 56 0.75mg/1 I) Cadmium 0.69 0.19 mg/I TCLP TCLP I] 2,4D1chlorophenoxyacetie acid (2,4-0) 0.72 10 II Methapyrilene 0.081 ,.s II Chromium (Total) 2.77 0.86 mg/l TCLP I) o.p·-ooo 0023 0.087 0.25 0.,0 [I Cyanioes (Total) 1.2 560 I [) p,p'-DDD 0.023 0.087 [I 3-Methylcholanthrene 0 0055 15 !] Cyaniaes (Amenable) 0.66 30 II o,p'-ODE 0.031 0.087 !l 4,4-Methylene bis(2-0 50 30 [J Fluoride 36 NA chloroaniline) 11 p,p'-DDE 0.031 0.087 I) Metnylene chloride 0089 30 II Lead 0.69 0 37 mg/I TCLP !l o,p'-DDT 0.0039 0087 11 Methyl ethyl ketone 0.28 36 II Mereury-Nonwastewater from NA 0.20 mg/I TCLP Retort I [J p,p'-DDT 0.0039 0.087 u Methyl ISObuty! ketone 0.14 33 II Mercury-All Others 0.15 0.025 mg/I TCLP [l DIben.z(a,h) anthracene 0.055 6.2 I) Methyl methacrylale 0.14 160 11 Nickel 3.98 50mgflTCLP II 01?>en.zo(e.e) pyrene 0.061 NA O Metnyl metnansulfonale 0018 NA [] Selenium 0.82 0.16 m;fl TCLP [I m-Dichloroberu:ene 0.036 6.0 {l Metr"lyl parathion 0014 ,.6 {I Sil~er 0.43 0.30 mgfl TCLP !] o-Oich!orooenzene 0.088 6.0 11 Na;mtnalel'\8 0.059 56 I} Su!fide ,. NA • {] p-D1chlorooenzene 0.090 6.0 II 2-Naphthylamine 0.52 NA 11 Thallium 1.4 0.078 mg/! TCLP I] Dichlorod1fluorome!hane 0.23 7.2 II o-N1troanihne 0.27 ,. U Vanadium ,.3 0.23 mg/I TCLP II 1 .1-D1chloroethane 0.059 6.0 II p-N11roaniline 0.028 26 II Zinc 2.61 5 3 mg/I TCLP I SECTION IV LAB PACKS EPA Code(s) I I I SECTION V CERTIFICATION I certify under penalty of law that I personally have examined and an familiar with the waste through analysis and testing or through knowledge of the waste to support this certificaztion that the waste complies with treatment standards specified in 40CFR Part 268 Subpart D and all applicable prohibitions set forth in 40CFR 268.32 or RCRA Section 3004(d). I believe that the information I submitted is true, accurate and complete. I am aware that there are significant penalties ;or submitting a false certification, including the possibility of a fine and imprisonment. I certify under penalty of law that I personally have examined and an familiar with the waste and the lab pack does not contain any waste identified in Appendix 4 to Part 268. I am aware that there are significant penalties for submitting a false certification, including the possibility of a fine and imprisonment. AutJto'rized Representative Signature Print or Type Name Date · 1 c,)-J -s0e:;r-f6-C,a,,12-1), ,v >-'r]l:,}~ Title I I CRISTEX DRUM SITE I DRUM# MANIFEST LINE ITEM PROFILE# CD-01 118 2-578 I CD-02 118 2-578 CD-03 118 2-578 CD-04 11A 1-426 I CD-05 11C 2-579 CD-06 11C 2-579 I CD-07 11A 1-426 CD-08 118 2-578 CD-09 118 2-578 I CD-10 118 2-578 CD-11 118 2-578 CD-12 11C 2-579 I CD-13 118 2-578 CD-14 118 2-578 CD-15 118 2-578 I CD-16 118 2-578 CD-17 118 2-578 CD-18 118 2-578 I CD-19 118 2-578 CD-20 118 2-578 I CD-21 118 2-578 CD-22 118 2-578 CD-23 118 2-578 I CD-24 118 2-578 CD-25 118 2-578 CD-26 11D 6-216 I I I I r~y I I I. .I UNIFORNl°HAZARDOUS WASTE MANIFEST Emergency Contact Telephone Number 1. Generator's US EPA ID No. Manifest Document No. N·C·O·O·O· 1·6·0·6·2·5·0 9.3.7. 1-7 3. Generator's Name and Mailing Address USEPA/W~D/{RRB -·.CRISTEX SITE ATTN: HR{!,TONY MOORE, DSC 100 4. Gene,ato,'s Pho~~J.:-. 404 ) 562_9756 ALABAMA ST.,SW.llTH FLOOR ATLANTA. GA 30303 5. Transporter 1 Co~any Name V':'_!~"1.! MCF SYSTEMS,ATLANTA 7. Transporter 2 ComPany Name . ,t' INC. 9. Designated Facility Name and Site Address MKC ENTERPRISES, INC. 5856 New Peachtree Rd DORAVILLE. GA 30340 6. US EPA lD Number G-A·D-9-8-1·2·6-9-0-9-5 8. US EPA ID Number 10. US EPA ID Number G·A·D·0·0·0·6· 1·6·3·6•7 of A. 93717 B. State Generator's ID NC0001606250 C. State Transporter's ID D. Transporter's Phone ( 770) 593-9434 E. State Transporter's ID F. Transporter's f='.hone G. State Facility's ID GAD000616367 H. Facility's Phone (770 l 11. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number) HM 12. Containers 13. 14. a. X PRINTING INK, 3, UN1210, PG!! o. NON-REGULATED MATERIAL(BLACK ORGANIC SLUDGE> NON-REGULATED MATERIAL,<AQUEOUS LIQUID) d. X HAZARDOUS WASTE, LI QUID, N. 0. S., (LEAD l, 9, NA3082, PG I I I No. Type 02-D·M 2.1 D·M oz_ D·M C?I D·M Total Unit I. Quantity Wt/Vol Waste No. Est. DOOl 8co p Est. NRM 8'tOO p Est. NRM Boo p Est. D008 '-too p Additi_onal Desc~ptions for Materials-Listed Above K. Handling Codes for Wastes Listed Above 11AlM1084/1-426. 11DlM1084/6-216 11 B lM 1084 /2-578 UC )Ml 084/2-579 CRISTEX DRUM AND SUPERFUND S !TE: OXFORD, NC 15. Special Handling Instructions and Additional Information If spill occurs, refer to ER Gui de It's a) 129 b ) c ) d ) Guidebook: 171 (provided in vehicle) 24-Hour Emergency Response# (770) 457-1341 16. GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway according to applicable international and national governmental regulations. 18. 19. U I am a large quantity generator, I certify that l have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present and future threat to human health and the environment; OR, if I am a small quantity generator, I have made a good faith effort to minimize my waste generation and select the bes! waste management method that is available to me and that I can afford. Printed/Typed Name ~'2.£-- Siit~re Month el ,.i,-e,..t-~s 3 P,inted/fyped~a'J-/ Signature Month Day d .;i Transporter 2 Acknowledgement of Receipt of Materials Printed/Typed Name Signature Month Day Discrepancy Indication Space 20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest e pt as noted in Item 19. ORIGl~'AL -RETURN TO GENERATOR I MAR-19-97 ~ED 16:20 8ft BFI 10 complete this area. BFI Initiator: OHM CORP ERGS GOVT SERVS FAK NO, 40472$7200 P, 02 BROWNING-FERRIS INDUSTRIES WCONO AZ 2465 I I I BFI WASTE CODE WASTE APPROVAL REQUEST Action Requested: •-:-' New Waste Approval Location: ______________ _ C: Up-Date Approval -Previous Number: Company Number: ____________ _ Disposal Sita Requested: ________ ............. . Telephone: ( Fax: ( Date: -· .. Company Number: Management Method Requested: C: Lancifill r, Hau·,ing C: Other: WASTE CHARACTERIZATION DATA SPECIAL WASTE IMPORTANT: INFORMATION FOR PHYSICAL COMPLETION OF THI$ FORM MUST SE OBTAINED FROM AN AUTHORIZED REP-RF.SF:NTATIVE OF THE WASTE GENERATOR. PLEASE READ THE INSTRUCTIONS BEFORE COMPLETING THIS FOR!~. THIS FORM IS TO BE USED ONLY ONE TIME, AND MUST BE TYPEWRITTEN OR LEGIBLY PRINTED IN INK, A"JD SIGNED. I ! -·-·•·· ______________ ,_· G_E_N_E_R_A_T_O_R_IN_F_O_R_M_A_T_IO_N ___________ ~ __ _, I a) Generator's Name: USE PA ¾1 C>ly 'JY' bl G€neraling Facility's Address: C ,is~ Si½., Ci1y: 0)(.~,c.Q_ Siate NC.Zip :;)...75~5 Industry Description/SIC Code: e) State/ProvinciallLocai Registration No.: -...,.---, · Generator's EPA Id. No.: Jt(:._~~<P lC., g, ~ 'l-5' 'f: ,, IJC\<\ I . ! 1 c) Generator's Representative: ·Tol-J '/ moo f'e_ Billing Information I I· Title: t) .";:..e-f!A. o\.l ·S<e~'!NfC.oc,1"~~!?,r f) Customer'sfJame: TP.lephone: ( 'it>'-/ ) ~ ?-. -g "7 5'.'? C, OPTIONAL FORM 99 (7-90) I Fax: (<./O'i ) 5~ -BG.. 15 OHiY\ v,r-r:Q ,.o.. +io N ) · · · · ~ ~s-T~ !<>,~•Jci .. ~I<...,.,_ )1 · -FAX TRANSMITTAL d) Emerg.ency/lnforrnation Contact: ..)OYY\ ?--~i,. To s,,. # of pages ► "2,_ From Tr.1e: TltD (),pQ;Q.t"r.a,~ r E: M-.ee I I Telephone: (7?c>) 45"?,. 7~49 Pho""st,,1.. -T1<,•(,,, t-1-------~---2-. G_E_N_E_R~A-L V 9 ~=-=-:;:-:~=1.-:-/90---j,F~.,:,,.EJ.~::.!_]2~-- I ~ ~S-N 7540-01-317-7368 5099_101 a) Name/Des.criptlon of the Waste: N-Ok.J -~--'•=-'--'---~ __ _ GENERAL seRvrces ADM1N1STRAT10N _ , C.or-4:tflr,,0<\~,Q. , • ?t'-t-V"\ 1'!== u;:, F1.::ieJ c i \ ~--~i t0 ~,· '?S .. ~'ok-I I I I I .I I b) Process Genera!ing the~aste: :€,J<:.C~'-10,..'.iio t\/ O~ 60 r ie.cQ s;> r u r----!:) --\: ~+···· , (ON"t"o,..'.~~ "ffCa r0"€..l oi \ '5u )w 0CW ?r1't..'.)-\-i ~ • "1:~"M~~~~~~t.~~ Mtlt.e& ~.-+:½, bl .,QQ.i-:\)~-~r.~_9,,._ ' c) Is ttus waste a charaetenstically hazardous waste as per 40 CFR 261.21-24? O Yes !:1J6 ,~ N/D d) ls this waste an F,K,P, or U listed hazardous waste as per 40 CFR 261.32-33? :; Yes ,~ = N/0 e) Is this waste a treatment residue of a waste wh;ch was previously a characteristically hazardous waste? CJ Yes ~ U N/D If yes, descrtbe the waste, applicable code(s), and the process generat;ng the waste prior to treatment. _______ _ f) Is this a "Hazardous Waste" as defined by State, Provincial, or Local Fiegulalions' CJ Yes ;?a = NJD If yes, enter the Waste Identification Number if one h~s been assigned:-------------,------ g) Recommended personal protection equipment and special handling procedures; · %lc.'-le. "::, j $ W TD e b 00:t'.:> D D DI D I I I ' NAR-19-97 WED 16:21 OHM CORP ERCS GOVT SERVS FAX NO. 4047297200 I SFI WASTe COOE / 3. WASTE PROPERTIES AT 72'F a) Physical State: i;?Solid O Semi-solid O Powder O Free Liquid , .• como:nation I P. 03 I b) Reactivey: 0 Water Reactive O Acid Reactive O Alkaline Reactive c O>cidi2er □ PyrO!)horic C Explosive C Toermally Sensitive CJ Shock Sensitive 0 Au~meri2able Cir1'fono o1 tho above c) Flash Point 'F: _,/ Cs 72 0 73-100 C 101-140 0 141•20C O l!: 201 il.1'1!A C N/0 d) pH: / Ss2 O2.1-5.0 C!".'5-1-9.0 C9.1 •12.4 0 ;,12.s :JNIA '.:N/D e) Odor-describ_.!l,-Pe---\-ral~t.,I""". u r-½,, / \?r, .:i+,\& soh:i<W+-.5. C None 2'Mild iJ Strong t- 4. WASTE COMPOSITION Please provide a breakdown of the waste stream based upon generator knowledge of the waste and the process(s) generating the waste stream. - 00"'3 this waste contain any of the following: 0 Free Cyanide 0 Free Sulfide ~anic Solvents 0 OSHA Substances 0 Radioactive Materials ~Oils w Used Oils :J Etiological Agents Components/Contaminants 5oi \ If the waste is a DOT Hazardous Material, com~:ete 11",e follow,ng: Range (o/o) GO -~Oo/21 ID -';36°fo Proper USDOT Shipping Name: ------'---------------------------I 1--u_s_o_o_T_H_az_a_rd_c_1_as_s_, :=.::::::::::::_u_N_a_r_N_A_N_u_m_b_er_. ::::;:_-_-_::_-_-___ -_:-___ c_e_R_c_LA_R_e_po_rta_o_1e_o_u_a_n,_i1y_: _-_-_-_::_-_-_-_-_-_ 6. GENERATOR'S CERTIACATION I I I hereby certify that the above and attach~ descrtpf.on is complete and accurate to the best of my l<nowledge and ability to determine, that no daliberate or willful ol'l"lissions of eompoc,ition or properties exist. that all known or suspected hazards have b~en disclo$ed, analytical result$ submitted are aecure,e and representative of-the waste (per SW846), and that the waste is not a regulated haz-ardous waste by the USEPA, by an applicable State or Provincial authority, or by any applicable local authority, and does not contain PCBs regulated by TSCA (i.e., 40 CFR 761) °' any Provincial authority. 1ENERATOR'S l)UTHC,RIZE0 SIGNATORY: DATE: 3/11 I 99: . r, ,r u ,1, •L;:t-~.,_\ , PRINT NAME: 'DE ~'11::\J!?NEµS Qrx>lleSIGNATURE: ,.CW ~~mu: TELEPHONE:( "4-04 ) £~z._-'?7t;;c,, FAX:( '-[o'-f) (~z.-fjG,,qq . I I I I I I I I I I I UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION 4 ATLANTA:FEDERAL CENTER 100 ALABAMA STREET, S.W. ATLANTA, GEORGIA 30303-3104 Ref I J FEB 2 6 1997 4WD-ERRB R_ECEIVED Mr. Jack Butler, Deputy Director Solid Waste Management Division North Carolina Division of Solid FEE .2 cl i9S7 Waste Management P.O. Box 27687 SUPERFUND SECTIO~' Raleigh, N.C. 27611-7687 SUBJ: Cristex Drum, Oxford, Granville County, North Carolina Dear Mr. Butler: The U.S. Environmental Protection Agency's Emergency Response and Removal Branch (ERRB) conducted a site investigation for potential removal action eligibility under the National Contingency Plan (NCP) at the above referenced site. Cristex Drum is located in Oxford, Granville County, North Carolina. The site is an abandoned drum dump containing an unknown number of drums, buried throughout a one-acre parcel. Various drums of characteristic hazardous waste include solvents and adhesives. Based upon the OSC's assessment, the site has been designated as a high priority for a removal action. This determination is based on observations that the site is completely unsecured and the proximity of the site to an adjacent neighborhood may pose a significant threat of possible exposure. OSC De'Lyntoneus Moore has been assigned this site. removal action was initiated on January 8, 1997. A copy Action Memorandum outlining the site threats and removal activities is enclosed. A of tJ:-,c Should you have any questions concerning ERRB's determination or actions, please contact De'Lyntoneus Moore, On- Scene Coordinator, at (404) 562-875 or Michael Norman, Chief of R=ovnl Qperncions SecCion, nc (404ce:i@t,,,.---- ~'Myron D. Lair, Chief Emergency Response and Removal Branch Racycled/Recyclable • Printed with Vegetable 011 Based Inks on 100% Recycled Paper (40% Postconsumer) I I I I I I I I I I I I I I I I ,. UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION 4 ACTION MEMORANDUM DATE: ATLANTA FEDERAL CENTER 100 ALABAMA STREET, SW. ATLANTA, GEORGIA 30303-3104 RECEIVED FEB 2 8 1997 SUPERFUND SECTIO~I SUBJECT: Request for a Removal Action at the Cristex Drum Site, Oxford, Granville County, North Carolina FROM: De'Lyntoneus Moore, osc~ TO: Richard D. Green, Acting Director Waste Management Division I. PURPOSE The purpose of this Action Memorandum is to request and document approval of the proposed removal action described within for the Cristex Drum Site in Oxford, Granville County, North Carolina. II. SITE CONDITIONS AND BACKGROUND The Cristex Drum Site (hereafter referred to as "the Site") is an unauthorized dumping ground for an unknown number of buried drums. During the course of the Site investigation, five (5) intact drums were uncovered at the Site. Due to the deteriorated condition of the drums, three of these drums ruptured during the trenching operation. Field test indicated that at least one drum contained a chlorinated oil of at least 50 ppm of a chloride compound. The site location is accessible and adjoins a nearby apartment complex: Ownership of the Site is unknown at this time. The area appears to be located within the right-of- way of the local utility company. The total project ceiling for the planned removal activity is $223,500 of which $150,000 will be used for the ERCS contractor. Recycled/Recyclable e Printed with Vegetable Oil Based Inks on 100% Recycled Paper (40% Postconsumer) I I I I I I I I I I I I I I I I I I I A. Site Description 1. Removal site evaluation The abandoned drums were buried in the area by an unknown party at an unknown date. The Site was identified the by North Carolina Department of Health, Environment, and Natural Resources (DHENR) through their work at an adjacent NPL Site. Drums are scattered in two distinct clusters with individual drums radiating from each cluster. Some drums are partially or completely buried. It is suspected that more drums are buried under the visible drum clusters. The condition of the drums ranges from intact to extremely deteriorated. 2. Physical location Approximately 1,000 residents live within a two mile radius of the Site. Private wells have not been identified at this time. 3. Site characteristics It is possible that closed Cristex. facility. unknown at this time. the Site is connected with the Former plant operations are 4. Release or threatened release into the environment of a hazardous substance, or pollutant or contaminant Field test revealed that the drums may contain a chlorinated compound. The stability of the binding matrix is unknown. It is also not known how fast the compound degrades.and disperses into the soil and/or water. The contents u:: many of the drums in the area cannot be identified at this time. The exact numbers and quantities of all wastestreams present are unknown at this time. 5. NPL status This site is not on the NPL nor is it expected to attain a rating sufficiently high enough to make the NPL. B. Other Actions to Date 1. Previous actions None I I I I I I I I I I I I I I I I I I I 3 2. Current actions Currently, there are no governmental or private clean' up efforts occurring at the site. C. State and Local Authorities' Role 1. State and local actions to date None. III. THREATS TO PUBLIC HEALTH OR WELFARE OR THE ENVIRONMENT, AND STATUTORY AND REGULATORY AUTHORITIES A. Threats to Public Health or Welfare The EPA Region 4 ERRB has determined that a release threat, as defined by Section 101 of CERCLA, exists at the Site .. The Site meets the requirements for initiating an immediate removal according to the criteria listed in Section 300.415 if the National Contingency Plan (NCP). The nature and behavior of the substances on-site are unknown. It io not known if the·se drums. orig.inated from the Cris tex facility. Further deterioration of the drums on-· site will allow a continued release of suspected hazardous components to the environment. The Site is unsecured.and accessible to the public. Based on the existing conditions at the Site and the evaluation of the potential risks posed by the drums, the following factors cited from the NCP were· considered in determining the appropriateness of a removal action: 1) 2) Section 300.415 (b) (2) (iii) "Hazardous substances or pollutant or contaminant in drums, barrels, tanks, or other bulk storage containers, that may pose a threat of release", Section 300. 415 (b) (2) (i): "Actual or potential exposure to nearby human populations, animals, or the food chain from hazardous substances or pollutants or contaminants", and 3) Section 300.415 (b) (2) (iv): "High levels of hazardous substances or pollutants or contaminants in soils largely at the surface, that may migrate". No Potentially Responsible Parties (~RPs) have been identified for this Site. It is not expe~ted that the PRPs, if found, will respond and perform a remc.. ·al in a timely manner. It is not expecte::1 that the Stat,, or any other I I I I I I J 4 governmental entity will conduct the necessary remediation activity. Subsequently, the following cite from the NCP was considered: B. Section 300.415/b) /2) /vii) "Availability of other appropriate federal or state response mechanisms to respond to a the release" . Threats to the Environment As previously stated, the nature and behavior of the hazardous substances on-site are unknown. It is not known if these drums originate from the Cristex facility. Further deterioration of the drums on Site will allow continued release of hazardous components to the environment. I IV. ENDANGERMENT DETERMINATION I I I I I I I I I I I I V. Actual of threatened releases of the hazardous substances from this Site, if not addressed by implementing the removal action selected in this Action Memorandum, may present an imminent and substantial endangerment to the public health or welfare or the environment. PROPOSED ACTIONS AND ESTIMATED COSTS 1. Proposed action description EPA's proposed actions at the site can be divided as follows: Phase I Excavate, consolidate, and stage all drums found on- site for sutsequent sampling. Sample all wastestreams to determine the disposal requirements .. If necessary, treat the contaminated water on-site. Remove the contaminated soil and sediment in the area of concern. Phase II Dispose of all wastestreams by the appropriate measures as determined by the disposal profile. I I I I I I I I I I I I I I I 5 2. Contribution to remedial performance Based on the information available at this time, the proposed removal activity will abate the immediate threats identified in Section III of the this document. If further remedial actions are necessary due to the presence of groundwater or other contamination, then the proposed action will remove the primary sources of groundwater contamination and aid in the long term clean-up goals. 3. Description of alternative technologies Because the final disposition of the waste materials at the site has not been determined, no formal evaluation of alternative technologies has been made. Such an evaluation will take place before the disposal phase of the response action and will be documented at that time. 4. Applicable or relevant and appropriate requirements (ARARs) Federal ARARs determined to be practicable for the site are the Resource Conservation ana Control Act (RCRA) and possibly Toxic Substances Control Act (TSCA). At this time the State of North Carolina has identified no substantively additional ARARs. 5. Proposed Schedule Response actions at the site will be initiated upon approval of this Action Memorandum. Foregoing any unexpected delays, all actions are expected to be completed within one year of mobilization. B. Estimated Costs Extramural Costs Regional Allowance Cost ERCS Non-Regional Allowance Cost START Subtotal 15% Contingency Total, Extramural Cost $150,000 20,000 $170,000 $25,500 $195,500 I I I I I I 6 Intramural Cost Direct (333 hrs at $30.00) Indirect (333 hrs at $54.00) 10,000 18,000 Total, Intramural TOTAL SITE BUDGET $28,000 $223,500 VI. EXPECTED CHANGE IN THE SITUATION SHOULD ACTION BE DELAYED OR NOT TAKEN If action is significantly delayed or not taken there will continued release into the environment increasing the possibility of exposure to the public. VII. OUTSTANDING POLICY ISSUES I NONE I I I I I I I I I I I VIII. ENFORCEMENT At this time there are no identifiable potentially responsible parties (PRP) that may undertake response actions. If additional information becomes available during the removal action, appropriate enforcement activities will be taken. IX. RECOMMENDATION This decision document represents the selected removal action for the Cristex Drum site in Oxford, Granville County, North Carolina; developed in accordance with CERCLA as amended, a~d consistent with the NCP. Conditions at the site meet the NCP section 300.415(b) (2) criteria for a removal and I recommend your approval of the proposed removal action. The total project ceiling if approved will be $223,500. Of this, an estimated $150,000 comes from the Regional removal allowances. Approval=--'-'~'--"--,.._.,;..,· --'--1---"--' 1 "-~=--'-'0"-. "-~-=---·---- ;~ Disapproval: _________________ _ cc: Jack Butler, Chief Superfund Section NC Division of Solid Waste Management Date: IZ/2/")l, I ; Date: _____ _ " f'.\ ./, I I I I I I I I I I I I I I I I I I •• Phase I Environmental Audit Cristex Corporation Oxford, North Carolina March 1, 1991 Prepared For Cristex Corporation Butner, North Carolina Prepared By Aquaterra, Inc. Raleigh, North Carolina Ref 12 RECE\VELj JJJN, 2 5 1998 81.lPERFUND SECTION ,A-,-· Aquaterra, Inc. ~ I I I I I I I I I I I I I I I I I I ~·~ .. ~ 4 AQUATERRA. ~ Environmental Consultants March 1, 1991 Cristex Corporation 26th and C Street Butner, North Carolina 27509 Attention: Mr. Bill Bruce Vice President Reference: Phase I Environmental Audit Cristex Corporation Oxford, North Carolina Aquaterra Job No. 550 Dear Mr. Bruce: Aquaterra, Inc. (Aquaterra) is pleased to present this Phase I environmental audit of the Cristex Corporation (Cristex) facility located in Oxford, North Carolina. Aquaterra's approach to performing this environmental evaluation consisted of two phases of work. The first phase included reviewing the available public record regarding the ownership history, available aerial photographs and topographic maps of the site; and information regarding past, present, or pending enforcement activity related to environmental regulation. The North Carolina Department of Environment, Health, and Natural Resources (NCDEHNR) was contacted and a formal request to view available pertinent files was requested under the Freedom of Information Act. Environmental files were reviewed in both the regional and central NCDEHNR offices. The second phase of work consisted of an on-site reconnaissance of the property for visual indicators of possible deposition, use, and/or storage of hazardous materials. The reconnaissance also included a survey to inventory and note adjacent properties that could potentially contribute to adverse environmental impacts to the Cristex parcel. To acquire much of the historical information contained in this report, an interview with Cristex personnel was conducted. This report, to the best of our knowledge, accurately represents existing and past environmental conditions at the subject property based on the information contained in the public record and site conditions at the time of our evaluation. If conditions at the site differ or change from the conditions detailed in this report, we request that Aquaterra be contacted so that these changes can be properly reviewed and our report amended accordingly. Corpou.tc. Office: POBoi,;Sill28 Raleigh. NC 27650 {919) 859-9987 FAX (919) 859-9930 O,ulotte Office: ro Box 668101 Chulotte, NC 28266-81CJ7 (704) 525.USO FAX (704) 527-2792 Cret'ruboro Offke: POSair. 16241 GJ"Ci!mboro, NC 27416--0241 {919) 27.J.5003 FAX (919) 271-8138 IJ I I I I I I I I I I I I I I 'I I I I Cristex Corporation R1261-91 March 1, 1991 Page 2 If you have any questions concerning this report or if we can be of any further assistance, please contact us at (919) 859-9987. Senior Peer Review: ~~¥\~ Phillip L. Rahn, P.G. ~ President KBP/rndy Sincerely, AQUATERRA, INC. ffJ.h /Jt>l!Md Kirk Pollard Project Manager Aquaterra, Inc. ® I I I I I I I I I I I I I I I I I I 1 2 3 4 5 6 Contents Introduction Review of Property Ownership, History, and Public Record 2.1 Chain-Of-Title Examination 2.2 Local Officials and Contacts 2.3 Solid and Hazardous Waste Agency Contacts 2.3.1 RCRA List Review 2.3.2 CERCLA and Superfund List Review 2.3.3 Solid Waste Management File Review 2.4 Division of Environmental Management 2.4.1 Ground Water File Review 2.4.2 Water Quality File Review 2.4.3 Air Quality File Review 2.5 Surficial Geology 2.6 Aerial Photographs and Topographic Map Examination Site Reconnaissance 3.1 Physical Setting 3.2 Manufacturing Facility 3.2.1 Facility Description 3.2.2 Manufacturing Processes 3.2.3 Environmental Liabilities in Manufacturing Facility 3.3 Wastewater Surface Impoundment 3.4 Other Areas 3.5 Site Utilities 3.6 Septic Tanks, Leaching Fields 3.7 Surrounding Properties Conclusions Recommendations Limitations ll] 1 1 1 2 2 2 3 3 3 3 4 4 5 5 6 6 6 6 6 7 7 7 8 8 8 8 10 11 J¥~-- Aquaterra, Inc. ~~ I I I I I I I I I I I I I I II ' I I I I I Figure 1 Figure 2 Table 1 Table 2 Table 3 Table 4 Attachment A Attachment B Attachment C Attachment D Figures Site Location Map Site Map Tables Registered Underground Storage Tank Facilities POTW Discharge Analytical Results Asbestos Analytical Results Surface Impoundment Sludge Analytical Results Attachments DEM Air Quality Report and Inspection Forms Photographs Asbestos Analytical Results Analytical Results IV -·= a~~ Aquaterra, Inc. '-i:;J I I I I I I I I I I I I I I I I I I [I 1 Introduction Phase I Environmental Audit Cristex Corporation Oxford, North Carolina March 1, 1991 Aquaterra, Inc. (Aquaterra) conducted an environmental evaluation of the Cristex Corporation (Cnstex) property located in Oxford, North Carolina (see Figure 1). The original scope of work was outlined in Aquaterra Proposal No. P610-91 approved by Mr. Bill Bruce of Cristex. From 1968-86 the facility was primarily used to produce warp knitting textiles. Over this 18-year period, several dying acid compounds and other compounds were used to produce the manufactured products. In addition, deminimus quantities of solvent products were used to clean equipment. This audit was conducted to identify potential environmental liabilities from the previous site operations. 2 Review of Property Ownership, History, and Public Record Aquaterra reviewed available public records and interviewed individuals and public agency contacts knowledgeable of the property. This information was used to identify past or present activities at or near the site that might indicate the deposition of hazardous materials or violations of environmental regulations. The following summaries of waste disposal, hazardous waste, and permitting activities at the site were obtained from the public record and/or from representatives of local, state, and federal agencies. Information presented below was authorized by each contact for inclusion in this report or was available for public review. 2.1 Chain-Of-Title Examination A chain-of-title search was conducted at the Granville County Register-of-Deeds in Oxford. A review of the records indicated that two tracts of land were purchased on August 31, 1965, by Steinfield Mills: • an 11.13 acre track from John H. Nelms and wife Mary Ruth C. Nelms • an 11.28 acre track from Cinco Investors, Inc., George E. Daniel, J.K. Bryan, Jr., Louis R. Hutchinson, John E. Pittard, Jr., and J.K. Nelms These two tracks comprise the existing parcel. Steinfield Mill, Inc. changed its name to IMI Knits, Inc. on June 18, 1971, through an article of amendment. IMI Knits, Inc. changed its name to Cristex, Inc. on February 18, 1981, through another article of amendment. Cristex is the present owner. Page 1 of 11 Aquaterra, Inc. I 'I I I I I I I I I I I I I I I I I I 2.2 Local Officials and Contacts Cristex Corporation R1261-91 March 1, 1991 Aquaterra contracted the Oxford Fire Department, Central office, regarding any responses to fires, illegal dumping, or spills of hazardous materials responses at or near the site. According to Mr. John Norris, Chief, the department had responded to fires in the exhaust stacks once or twice over the past several years. These incidents may have been caused by linen buildup. Mr. Norris also recalled a single dumpster fire caused by nearby welding activities .. Mr. Norris did not recall any incidents of illegal ct umping or spills on the site. Aquaterra contacted the Oxford Department of Public Works regarding any knowledge of utility repairs or problems associated with releases of hazardous materials into the municipal utility systems. According to Mr. Jimmy Crews, director of City Public Works, no reports of water supply disruption resulted from hazardous material releases on or adjacent to the site. Mr. Crews mentioned that Channel Master (J.F.D. Electronic Southern, Inc.), located adjacent to Cristex to the north, stopped discharging to the public owned treatment works (POTW) approximately 8 years ago. Aquaterra contacted Mr. Mitchell Bird of the North Carolina Emergency Management Division concerning site-specific responses to solid and hazardous waste releases, ground water contamination, leaking underground storage tanks (USTs), and other reported activities on or adjacent to the site that could potentially impact the site. No reports of such activities or any responses from that agency were on record during the 2-year existence of the agency. 2.3 Solid and Hazardous Waste Agency Contacts Aquaterra contacted the North Carolina Department of Environment, Health, and Natural Resources (NCDEHNR) regional and central office agency personnel regarding known facilities or sites currently monitored or regulated by state agencies due to environmental permits; known violations of environmental laws; or hazardous material disposal, s.torage, use, or releases at or near the site. The following information was obtained through interviews and file searches conducted at both offices. 2.3.1 RCRA Lisi Review Aquaterra contacted ·the Hazardous Waste Branch (HWB) for lists of Small Generators, Generators and Transporters, and Starers and Disposers of hazardous wastes, and materials covered under the Resource Conservation and Recovery Act (RCRA). The following RCRA regulated facilities are in close proximity to the site. EPA ID# NCD044389344 NCD052555315 NCD982080095 Facilitv Bandag, Inc Ideal Fastener Corp. Plastic Engineering Corp. Address Industry Drive Industry Drive 18D Industry Drive Page 2 of 11 Status Small Generator Generator Small Generator Aquaterra. Inc. ~I I I I I I I I I I I I I I I I I I I I --- 2.3.2 CERCLA and Superfund List Review Cristex Corporation R1261-91 March 1, 1991 Aquaterra requested data on known hazardous waste sites and facilities of known or potential sites of concern under "Superfund" legislation from NCDEHNR. Information collected from the Superfund Branch indicated that one Superfund site, Channel Master (previously JFD Electronic Southern, Inc.), is less than 1,500 feet north of the Cristex site. The Channel Master property has one surface impoundment and soil and ground water contamination are under investigation. Ground water generally flows to the southeast, which could possibly impact the site. 2.3.3 Solid Waste Managemelll File Review Files within the Solid Waste Section were reviewed for permits, notices of violations, consent orders, etc. issued to facilities for operating solid waste, open dumps, or demolition landfills. The files revealed that Granville County operates or has permitted two solid waste landfills. None of the sites disclosed are found with close proximity to the Cristex parcel. No other demolition landfills or open dumps are noted within the county or city. 2.4 Division of Environmental Management Aquaterra contacted 'the Raleigh Regional Office of the NCDEHNR, Division of Environmental Management (DEM) for information on State environmental permits regulating air and water discharges issued for the site and adjacent facilities. Agency personnel in the Ground Water, Surface Water, and Air Quality Sections provided information and technical assistance regarding relevant information contained in the environmental files. 2.4.J Ground Water File Review Incident Repons Ms. Fay Sweat with the Regional DEM Groundwater Section was visited for information regarding pollution incidents reports. The files contained two pollution incident reports for facilities located within 1500 feet of the Cristex site. The first was at Bandag, Inc. (505 West Industry Drive) where a UST line leak resulted in the release of virgin hexane. The leak was discovered on April 12, 1990, in a monitoring well adjacent to the UST. Ground water was impacted. Bandag repaired the pipe and began pumping free product from a monitoring well. A second pollution incident report was completed for Channel Master (613 Pine Tree Road) during a compliance investigation. The incident resulted from incomplete remediation of the on-site surface impoundment. Although soil cleanup had been performed, no ground water remediation had been initiated as of January 20, 1989. The type of pollutant noted was solid waste leachate and metals. A DEM memorandum dated October 20, 1989, stated that during a preliminary investigation of the surface impoundment area at the site during summer 1985 evidence of ground water contamination originating from multiple sources was noted. Data indicated that the halogenated and petroleum solvents contamination has entered the bedrock aquifer. A DEM memorandum dated July 1, 1986, stated Channel Master wished to "close" the abandoned sludge surface impoundment so Page 3 of 11 Aquaterra, Inc. ~ 11 ~ D I I I I I I I I I I I I I I I I Cristex Corporation R1261-91 March 1, 1991 that they may seal the property. "Deep well MW-5, screened from 45 to 55 feet, showed the presence of trichloroethene, tetrachloroethene, and toluene. A source other than the surface impoundment was responsible for the solvents in the ground water. A reconnaissance of the site using a hand auger indicates that a septic tank formerly used as a UST is the source." Underground Storage Tanks The file review revealed that several facilities within a 1,500-foot radius of the site currently operate registered USTs (see Table 1). Of those facilities listed, none have reported product loss or releases, except those noted above. Additionally, the file review indicated that no notifications of tank closure (30-day notice) have been submitted for sites located within a 1,500-foot radius. Water Supply and Monitoring Well Permit Issuance Review of the permit files indicate that apparently no permitted public or private supply wells exist within a 1,500-foot radius of the site. The closest facilities with monitoring wells are the Channel Master site and the Bandag site. 2.4.2 Water Quality File Review The Raleigh Regional Water Quality Section was contacted regarding National Pollution Discharge System (NPDES) Permits and Non-Discharge Permits issued for the site. It was determined that no NPDES or Non-Discharge Permits have been issued for the site. Publicly Owned Treatment Works (POTW) Permit The Cristex Corporation discharged its wastewater to the City of Oxford POT\V under Permit No. 0106. Table 2 contains analytical results of Cristex effluent to the POTW. A compliant filed with the Raleigh Regional Office, dated February 11, 1982, addresses a discharge of heated water to a ditch around the perimeter of the surface impoundment. Apparently, a waste line from the plant to the surface impoundment had broken and resulted in waste entering the ditch. Within 3 days, the flow was diverted into the surface impoundment. A new discharge line was apparently installed. 2.4.3 Air Quality File Review The Cristex Corporation is an air quality permitted facility currently operating under Permit No. 2097R4 (expires March 31, 1991). A DEM Air Quality Report dated March 21, 1983, (see Attachment A) noted an oil spill in the surface impoundment. The inspector also noted that although visible and particulate emissions were in compliance, he noticed a large amount of smoke inside the plant and was given no explanation. Page 4 of 11 Aquacerra, lnc. I I I I I I I I I I I I I I I , I I 2.5 Surficial Geology Cristex Corporation R1261-91 March 1, 1991 Review of the Geologic Map of North Carolina, 1985 edition, indicates that the site is located in the northern portion of the Piedmont Physiographic Province, Carolina Slate Belt. The bedrock consists of metamorphosed granite rock, Cambrian in age, which is generally megacrystic, and well foliated. 2.6 Aerial Photographs and Topographic Map Examination Aerial photography and the USGS map of the Oxford Quadrangle (dated 1981) were reviewed for this site. The USGS topographic quadrangle reveals the surface impoundments on both the Cristex and Channel Master sites. An apparent farm pond directly south of the Cristex site is also shown. Eleven photographs from eleven flights from 1961-83 were reviewed at the North Carolina Department of Transportation Photogrammetric Unit: M-123 M-393 M-471 CS-12 M-969 M-1366 M-1626 M-1656 M-1966 M-1670 M-1697 Exposure 734 Site Outside Mission Site Outside Mission Site Outside Mission Exposure 4 Site Outside Mission Exposure 16 Exposure 15 Site Outside Mission Site Outside Mission Exposure 98 3-20-61 2-5-64 4-3-64 9-9-68 11-15-68 3-15-78 9-23, 24-81 3-12-82 4-23-82 1-4-83 2-4-83 Mission M-123, Exposure 734 (3-20-61) shows the Cristex property and the surrounding properties as wooded farmland. No pond or surface impoundment exists on the Cristex property. Mission M-969, Exposure 4 (11-15-68) includes the Cristex and Channel Master plant buildings and surface impoundments. East of Cristex is wooded land, and other. plants and/or businesses are south and east. The scale of this photo is too small to distinguish significant detail. Mission M-1626, Exposure 16 (9-23,24-81) shows both Cristex and Channel Master facilities and surface impoundments. Wooded land still exists east of the site. Three large buildings exist to the south, and one large plant is to the west. A vacant lot is directly south of the site. Aboveground tanks and a possible drum storage area are located east of the Cristex building. A clearing east of the surface impoundment appears to have no vegetation. Mission M-1656, Exposure 15 (3-12-82)-appears the same as Mission M-1626. Page 5 of 11 ~~ -·~ Aquaterra, Inc. ~ :I I I I I I I I I I I I I I I I I Cristex Corporation R1261-91 March 1, 1991 Mission M-1697, Exposure 98 (1-4-83) is similar to the previous two photographs. However, Cristex surface impoundment appears half black and half light; this type of color variation generally indicates that petroleum product floating on the water surface. 3 Site Reconnaissance On February 10, 1991, a project geologist was dispatched to conduct an environmental evaluation of the facility as well as the immediate surrounding areas (see Figure 2 and Attachment B for photographs). 3.1 Physical Setting The site is located on the east side of Industrial Drive approximately 2 miles southwest of Oxford, North Carolina. The site is triangular in shape and encompasses approximately 22.4 acres of land. 3.2 Manufacturing Facility 3.2.1 Facility Description An approximately 150,000 square foot manufacturing complex is on the property. The facility is presently vacant and has not been used since 1986. The existing manufacturing facility is constructed with structural steel and sheet metal walls and roofing. The floor in the manufacturing area is primarily concrete and tile in the office area. The structure was divided into six primary areas: • office area • manufacturing area • boiler room • mixing area • laboratory • warehouse area 3.2.2 Manufacturing Processes Producing warp knitting textiles was the primary facility operation from 1968-86. Over this 18-year period, several dying acid compounds and other compounds were used. Synthetic and/or cellulosic fibers were used to dye and finish the product. In addition, deminimus quantities of solvent products were used to clean ·equipment. The wastewaters generated from the manufacturing facility, mixing room, and laboratory facility were discharged through a series of pipings to the retention surface impoundment. Discharges were emitted to the atmosphere via ventilation systems. The atmospheric discharge was regulated by a permit issued by the Air Quality Section of the DEM. Several inspection forms conducted by DEM are included in Attachment A. Page 6 of 11 Aquaterra, Inc. I I I I I I I I I I I I I I I I I 3.2.3 Environmental Liabilities in Manufacturing Facility Cristex Corporation R1261-91 March 1, 1991 Several small containers were identified in the boiler room area. The contents appear to be used as boiler cleaning compounds. Several areas in the structure exhibited tile floor and drop ceiling tiles. Samples of the material were collected from the laboratory area and were analyzed for the presence of asbestos by polarized light microscopy. Results indicated the ceiling tiles were comprised of 95 percent fibrous glass and 5 percent paint. However, the floor tile contained 2 percent asbestos (chrysotile) and 98 percent filler (see Table 3 and Attachment C). 3.3 Wastewater Surface Jmpoundment In addition to the manufacturing facility, a 0.5 to 0.75 acre retention wastewater surface impoundment has been in operation on-site since 1968. The surface impoundment is equipped with aerator devices used for treatment purposes. The unlined surface impoundment is bermed and is approximately 6 to 8 feet deep. The surface impoundment contains clear water with no evidence of suspended solids. The diking surrounding the impoundment appeared intact with no evidence of breaching. The surface impoundment has a discharge point for disposal to the nearby supplied manhole port. The effluent discharge was permitted by the local POTW. The permitted discharge was approximately 333,000 gallons per day. #6 fuel oil was accidentally released into the surface impoundment in 1986. The fuel oil was boomed and subsequently disposed of in accordance with state requirements. A single sludge sample was collected from the surface impoundment bottom with a hand auger bucket wrapped with tin foil. Sample portions were placed in prelabeled laboratory prepared containers. The samples were then placed in a cooler and chilled to 4° C and transported to a laboratory in accordance with chain-of-custody protocols. The samples were analyzed for the presence of total petroleum hydrocarbons (SW-846 Method 3550) volatile and semivolatile organic compounds (SW-846 Methods 8240 and 8270), and RCRA metals (SW-846 Method 6000/7000 series). Results are summarized in Table 4 and Attachment D. Based on previous sampling events conducted to maintain compliance existing POTW permit, additional sampling of the impoundment waters conducted at this time. 3.4 Other Areas with an was not Two aboveground storage tanks (ASTs), one 20,000 and one 30,000 gallon capacity, were identified at the site. These tanks are used to store #6 fuel oil for the boiler system. The ASTs are located on the eastern side of the building adjacent to the boiler room. Concrete diking was not present (see Attachment A). Visual staining was evident around the tanks, and reports indicate approximately 500 gallons of fuel were released and entered the surface impoundment via wastewater lines. Page 7 of 11 Aquaterra. Inc. ~.f!? ~ = I I I I I I I I I I I I I I I I I I I • Cristex Corporation R1261-91 March 1, 1991 An approximately 500 -750 gallon vat was identified at a separate location on the eastern side of the complex. The vat was reportedly used to capture blow down from the boiler and operational equipment. The vat was full with what appeared to be collected precipitation with an oily substance floating on the surface. A system of valves and piping appeared to discharge into a nearby drainage swale that was graded to the surface impoundment. The valves appeared to be in the off position. Staining was evident around the vat. Three drums adjacent to the vat appeared to contain contents similar to the vat. Approximately 50 -75 containers were noted on the eastern property boundary. Most of the drums were lying on their sides, but some contained liquid that appeared to be rainwater. Most of the containers were just off the Cristex property line. However, approximately 10 containers were located on the Cristex property. 3.5 Site Utilities The site is presently served by city water service. Carolina Power & Light provides power to the site. The primary source of heating for the manufacturing area was generated by a steam generated boiler system located in the boiler room. Fuel for the boiler system consisted of #6 fuel oil that was stored in two aboveground storage tanks located outside the building complex. Power needed for the manufacturing operation appears to have been supplied by natural gas. In addition, steam was also used in the manufacturing process. 3.6 Septic Tanks, Leaching Fields No septic tanks or distribution fields are located on the site. The site is served by city sewer. No spray fields, nitrification lines, or other waste disposal systems were observed at the site. 3. 7 Surrounding Properties The property is bordered to the north by railroad tracks and by heavy industrial facilities. Industrial Drive and light to heavy industrial facilities are south and west. The eastern property boundary is bordered by timbered woodland and a propane storage facility. Fencing encompasses the manufacturing area. The facility at Cristex's northern property line is listed on the Federal National Priority Superfund List. Laboratory results from samples collected at the monitoring wells at this site detected several species of volatile organic compounds (VOCs). 4 Conclusions Based on the file search results of the preliminary environmental audit, Aquaterra has the following observations regarding the Cristex property: • Review of the chain-of-title indicates that past owners were private concerns with no indication of past generation, storage, or disposal of hazardous wastes. Page 8 of 11 ~-r- Aquacerra. Inc. ~ I I I I I I I I I I I I I I I I I I • • • Cristex Corporation R1261-91 March 1, 1991 Review of the North Carolina Department of Transportation aerial photographs from 1961 to 1983 indicated conditions were similar to those that presently exist. Although previous indications of a petroleum spillage to the surface impoundment were noted (1983), sources indicate the release had subsequently been remediated. In addition, the site inspection did not reveal the presence of petroleum product floating on the impounded waters. In review of the public records, Aquaterra found no evidence in files of HWS that the site has an EPA identification number, which would indicate generation of hazardous waste. However, three nearby facilities have EPA identification numbers under RCRA: Bandag, Inc., Ideal Fasteners Corporation, and Plastic Engineering Corporation. Channel Master is a CERCLA site. Facilities in the vicinity of Cristex having USTs or have had USTs include Bandag, Inc., Channel Master, General Processors, Inc., Ideal Fasteners Corp., Oxford Printing and Finishing, and Rosemart #8. It is beyond the scope of this investigation to determine whether these USTs would impact the subject site. Based upon the on-site reconnaissance, the following conclusions are made: • • • • • No operations were being conducted inside the manufacturing complex . Laboratory analysis of the floor tiles detected 2 percent asbestos. No other apparent environmental concerns were identified. The two vertical ASTs on site contain #6 fuel oil for heating purposes. The tanks are situated on concrete pads but are not contained by any type of diking. Piping runs from the tanks, above grade, directly inside the building. Although surface staining is evident, it is isolated to a limited extent around the tank area. An approximately 0.5 to 0.75 acre bermed surface impoundment is located northeast of the building. No dike breaching was observed at the surface impoundment. The impoundment contained water free of suspended solids, and approximately 1 to 2 feet of freeboard were noted. No discharges from the manufacturing area were observed. An approximately 500 -750-gallon capacity vat was identified on the eastern side of the complex. The vat appeared to be full, with contents exhibiting an oil and water mixture. A system of pipes fed a nearby swale which was graded in the direction of the impoundment. Staining was evident around the vat and three drums were adjacent to the structure. Approximately 75 empty drums were identified on the eastern property boundary. Approximately 10 drums were not covered and were full of rainwater. The condition of these containers was fair to poor with obvious pitting and holes. The facility at Cristex's northern property line is listed on the Federal National Priority Superfund List. Laboratory results from samples collected at the monitoring wells at this site detected several species of VOCs with a component of ground water flow to the southeast toward the subject site. Page 9 of 11 ,/; ·;-=-- Aquaterra, Inc. '-v I I I I I I I I I I I I I I I I I I • 5 Recommendations Cristex Corporation Rl261-91 March 1, 1991 The following items are recommended for the environmental concerns mentioned in this report: • • • • • The asbestos containing floor tiles should either be removed and disposed of at a certified landfill or testing should be conducted to verify the air quality in the building. The two AST systems present some risk of release of petroleum product to the environment. The need for the two tanks should be reviewed. If this review indicates the need to continue operations, then the tanks should be encapsulated in a concrete-lined and diked containment structure. Due to observed surface spillage, it is recommended that a limited soil assessment be conducted to determine the impact to the underlying soils. The on-site surface impoundment was in use from 1968-86 and received wastewaters from the manufacturing area. The impoundment is a non- permitted unit; however, the effluent from the impoundment is permitted by the City of Oxford. Analytical results from the sludge sample revealed the presence of petroleum product in the form of #2 fuel oil at a concentration of 790 mg/kg. Samples results for volatile and semivolatile compounds indicated the presence of several organic chemical constituents, including chlorobenzene, ethyl benzene, toluene, xylenes, bis 2-ethylhexyl phthalate, 1,3-dichlorobenzene, 1,2-dichlorobenzene and 2-methyl napthalene at concentrations between 440 and 27,000 µ,g!Kg. Analysis for total metals indicated the presence of chromium (37 mg/kg) and total lead (8.6 mg/kg). Based on the analytical results, Aquaterra recommends remediating the sludge and assessing the underlying soil for VOCs, semivolatiles, and TCLP RCRA primary metals. The impoundment should then be backfilled. The remediation program should consist of either the removal of contaminated sludges or in place treatment. In addition, Aquaterra recommends installing a single monitoring well topographically downgradient of the impoundment area. The well should be installed to intersect the ground water table to allow sampling of the shallow ground water zone to determine if impacts to the ground water have occurred as a result of leaching from the bottom of the surface impoundment. The well would be sampled for purgeables (VOCs), base/neutral/acid extractables (semivolatile organic compounds), and total RCRA metals (eight metals). Aquaterra recommends sampling the contents of the vat on the eastern side of the property. Proper disposal of this material can be determined based on the analytical results. The stained ground around the vat and the drainage swale initiating at the discharge end of the pipe from the vat should also be characterized by limited surface soil sampling. Page 10 of 11 ,1-~•-· Aquaterra, Inc. ~ I I I I I I I I I I I I I I I I I I I • • 6 Cristex Corporation R1261-91 March 1, 1991 The abandoned drums identified on the eastern property boundary should be collected, crushed, and properly disposed. The drums containing liquids, apparently rainwater, should also be properly disposed. Limited surtace soil sampling is recommended in this area, after the drums are removed, to characterize any possible releases of petroleum or hazardous compounds to the soil. Limitations The work performed in conjunction with this study and the data developed are intended to describe information available on the specified dates and locations. This report does not warrant against future operations or conditions, nor does it warrant against operations or conditions present of a type or at locations not investigated. Aquaterra has based its assessment upon prior site history through interviews, available records, and conditions and activities observable during a physical site inspection. This report is not intended to determine whether or not soil or ground water contamination or waste emplacement may exist at the site. Such determinations would require comprehensive subsurface exploration and sampling acti,~ties, which were beyond the scope of services for a Phase I environmental site assessment. Page 11 of 11 Aquaterra, Inc. ~ I I I I I I I I I I I I I I I I I I I Table 4. Surface lmpoundment Sludge Analytical Results, Cristex Corporation, Oxford, North Carolina. Parameter Results GC/MS Purgeables by SW-846 Method 8240: Chlorobenzene Ethylbenzene Toluene Xylenes (Total) Base/Neutral Extractables by SW-846 Method 8270 Bis (2-ethylhexyl) phthalate 1,3 -dichlorobenzene 1,2 -dichlorobenzene 2 -methylnaphthalene RCRA Metals Arsenic Barium Cadmium Chromium Lead Mercury Selenium Silver (J) = Estimated value below quantitation limit Laboratory: Industrial & Environmental Analysts, Inc. Cary, Nonh Carolina Aquaterra Job No. 550 R1261-91 2,300 µ,g/kg 6,000 µ,g/kg 440 µ,g/kg ( J) 27,000 µ,g/kg 12,000 µ,g/kg 2,800 µ,g/kg ( J) 3,100 µ,g/kg ( J) 25,000 µ,g/kg <1.0 mg/kg <20 mg/kg <2.0 mg/kg 37 mg/kg 8.6 mg/kg <0.25 mg/kg <1.0 mg/kg <10 mg/kg ·I~ u~ m Total Petroleum Hydrocarbon Analysis IEA Sample No: 196-210-1 Date Received: 02-13-91 Client Sample No: S-1 Date Extracted: 02-14-91 Client Project No: 550 Extraction (SW 846 -3550) / GC-FID analysis (for #2 fuel oil,kerosene,varsol) Date Analyzed: 02-17-91 The sample contains a petroleum hydrocarbon blend with a distillation range similar to #2 fuel oil. The concentration is 790 mg/kg. The guantitation limit is 20 mg/kg. Comment: Quantitation limit elevated due to extract dilution prior to analysis. Extract diluted due to the presence of target compounds.