MO-88893_96869_CA_LSA_20230331

Phase I Limited Site Assessment

New South Tractor
977 and 985 US Highway 70
Newton, North Carolina

DEQ Incident No. 96869
H&H Job No. NST-001
March 31, 2023

Phase I Limited Site Assessment Information

Site Location:
977 and 985 US Highway 70
Newton, North Carolina

Site Owner:
Gunpowder Holdings, LLC
1948 Moss Dr., Newton, NC 28658

General Site Information:
Facility ID Number: N/A
NC DEQ Incident Number: 96869
Site Priority Ranking: anticipate low
Land Use Category: anticipate commercial/industrial
Latitude: 35.694650 N Longitude: -81.242119 W
Release Discovery Date: September 27, 2022
Estimated Quantity of Release: unknown
Cause/Source of Release: waste oil release from trench drain

I, Robert J. Cappleman, PG a Licensed Geologist at Hart & Hickman, PC, do certify that the
information contained in this report is correct and accurate to the best of my knowledge.
Hart & Hickman, PC is licensed to practice geology/engineering in North Carolina. The
certification numbers of the company are C-245/C-1269.
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Table of Contents

Section Page No.
1.0 Executive Summary and Recommendations ........................................................................1 
2.0 Introduction and Site History ................................................................................................4 
3.0 Receptor Information and Risk Characterization ...............................................................6 
3.1 Receptor Information .............................................................................................................6 
3.1.1 Water Supply Wells ........................................................................................................6 
3.1.2 Surface Water ..................................................................................................................6 
3.1.3 Subsurface Structures ......................................................................................................7 
3.1.4 Property Owners and Land Use ......................................................................................7 
3.1.5 Wellhead Protection Areas ...............................................................................................7 
3.2 Risk and Land Use Characterization .....................................................................................7 
4.0 Geology and Hydrogeology ....................................................................................................8 
4.1 Regional Geology and Hydrogeology ...................................................................................8 
4.2 Site Hydrogeology ..................................................................................................................8 
5.0 Soil and Groundwater Sampling ...........................................................................................9 
5.1 Soil and Groundwater Sampling Methodology .....................................................................9 
5.2 Soil Sampling Results ..........................................................................................................10 
5.3 Groundwater Sampling Results ...........................................................................................11 
5.4 Conclusion and Recommendations .....................................................................................11 

List of Tables

Table 1 Summary of Soil Analytical Results
Table 2 Summary of Groundwater Analytical Data
Table 3 Summary of Contiguous Properties

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List of Figures

Figure 1 Site Location Map
Figure 2 Site and Sample Location Map
Figure 3 Contiguous Properties and Receptor Survey Map

List of Appendices

Appendix A Risk Classification and Land Use Form
Appendix B Water Supply Well Information Survey Forms
Appendix C Boring Log
Appendix D Low-Flow Groundwater Sampling Form
Appendix E Laboratory Analytical Report

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Phase I Limited Site Assessment
New South Tractor
977 and 985 US Highway 70
Newton, North Carolina
H&H Job No. NST-001

1.0 Executive Summary and Recommendations

This Phase I Limited Site Assessment (LSA) report documents assessment activities at The New
South Tractor facility located at 977 and 985 US Highway 70 in Newton, Catawba County,
North Carolina (Site or subject Site). A Site location map is included as Figure 1. The Phase I
LSA was performed in response to a Notice of Regulatory Requirements issued by the North
Carolina Department of Environmental Quality (DEQ) Underground Storage Tank (UST)
Section dated November 22, 2022.

The Site consists of one parcel of two contiguous parcels of land (Parcel ID Nos. 373110453053
and 37311045632) that total approximately 8.1 acres. The Site is developed with an
approximately 11,600-square foot (sq ft) industrial office/service garage building that was
constructed in 1962 and a roughly 4,800-sq ft storage/garage building that was constructed in the
early to mid-1960s. The Site is occupied by New South Tractor, a farm, construction, and lawn
equipment dealer. The remainder of the site consists of paved parking areas and driveways,
concrete loading and storage areas, gravel storage areas, and undeveloped land. A Site map is
provided as Figure 2.

On September 15, 2022, H&H performed Phase II Environmental Site Assessment (ESA) soil
and groundwater sampling activities at the Site to evaluate the potential for impacts from the
north-south oriented trench drain in the central portion of the service department. Soil analytical
data indicated the volatile organic compounds (VOCs) p-isopropyltoluene, naphthalene, and/or
tetrachloroethylene (PCE) and the polycyclic aromatic hydrocarbons (PAHs) 1-
methylnaphthalene, 2-methylnaphthalene, and/or naphthalene were detected above the Soil-to-
Groundwater Maximum Soil Contaminant Concentrations (MSCCs) in soil samples SB-3 and
SB-4. No detections exceeded the Industrial/Commercial MSCCs. Methylene chloride was also
detected at low concentrations that appear to be related to laboratory contamination.
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Groundwater analytical data did not indicate the presence of VOCs or PAHs at concentrations
that are below the North Carolina 2L Groundwater Standards (2L Standards). Phase II ESA soil
analytical data are summarized in Table 1, and groundwater analytical data are summarized in
Table 2.

Based on the Phase II ESA soil and groundwater data, it appears that a waste oil release has
occurred from the closed trench drain in the central portion of the service garage.

Land Use/Risk Characterization
As part of the LSA activities, H&H performed a site land use and risk characterization survey.
Municipal water is available to all properties within 1,000 ft of the source area. Water supply wells
were not identified within 1,000 ft of the source area. Two unnamed tributaries of Cline Creek
transect the southern portion of the Site.

The Site is currently zone Highway Business District (B-2) and general manufacturing district
(M-1). The properties in the surrounding area are primarily zoned business (B-2 and B-4),
manufacturing (M-1), and residential (R-20A). The nearest residence is located approximately
350 ft northwest of the source area.

Phase I LSA Sampling
On March 6, 2023, H&H oversaw the advancement of one LSA soil boring/temporary
monitoring well (SB-3A/TMW-2A) placed adjacent to the location of former soil
boring/temporary well SB-3/TMW-2. Samples SB-3 and TMW-2 showed the highest level of
impacts in soil during the Phase II ESA in September 2022.

Soil analytical results for sample SB-3A (0-2) indicate the presence of several petroleum-related
VOCs, semi-VOCs (SVOCs), C9-C18 aliphatics, and C9-C22 aromatics at concentrations above
the Soil-to-Groundwater MSCCs. The detection of total C9-C22 aromatics also exceeds the
Residential MSCC but is below the industrial/commercial MSCC. Total chromium and lead
were detected in sample SB-3A (0-2) and SB-3A (21-23) at concentrations that are consistent
with published background levels for North Carolina soil.
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Groundwater analytical results for sample TMW-2A did not indicate the presence of VOCs,
SVOCs, extractable petroleum hydrocarbons (EPH), volatile petroleum hydrocarbons (VPH),
lead, or chromium at concentrations above the 2L Standards or the Gross Contamination Levels
(GCLs).

Recommendations
Based upon the results of the Phase I LSA, H&H recommends that DEQ issue a risk-based No
Further Action (NFA) letter for the release incident. As part of the NFA, H&H will complete
public notice requirements and file a Notice of Residual Petroleum (NORP) based on the
presence of C9-C22 aromatics above the Residential MSCC. Based on the isolated nature of soil
contamination, H&H requests that an alternate NORP restricting disturbance of impacted soil be
approved to allow for future residential use of the Site. A map showing the estimated extent of
soil contamination will be attached to the NORP.
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2.0 Introduction and Site History

This Phase I LSA report documents assessment activities at 977 and 985 US Highway 70 in
Newton, North Carolina. A Site location map is included as Figure 1. The Phase I LSA was
performed in response to a Notice of Regulatory Requirements issued by the DEQ UST Section
dated November 22, 2022.

The Site consists of one parcel of two contiguous parcels of land (Parcel ID Nos. 373110453053
and 37311045632) that total approximately 8.1 acres. The Site is developed with an
approximately 11,600-sq ft industrial office/service garage building that was constructed in 1962
and a roughly 4,800-sq ft storage/garage building that were constructed in the early to mid-
1960s. The Site is occupied by New South Tractor, a farm, construction, and lawn equipment
dealer. The remainder of the site consists of paved parking areas and driveways, concrete
loading and storage areas, gravel storage areas, and undeveloped land. A Site map is provided as
Figure 2.

On September 15, 2022, H&H performed Phase II ESA soil and groundwater sampling activities
at the Site to evaluate the potential for impacts from equipment service operations and an
associated trench drain and wastewater discharge to a drainage ditch. A summary of the
assessment results is provided below.

 No obvious evidence of current or former USTs was identified during a ground-
penetrating radar (GPR) survey. The GPR survey also indicated that a closed trench
drain in the equipment service garage previously discharged waste fluids to a drainage
ditch in the western portion of the Site.

 Three soil samples were collected to evaluate potential soil impacts along the closed
trench drain in the equipment service garage, and one soil sample was collected near the
former location of wastewater discharge to the drainage ditch. Two groundwater samples
were collected to evaluate potential groundwater impacts from equipment services
activities and former waste fluid collection in the trench drain.
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 Field evidence of petroleum-related soil impacts was identified along the trench drain
during field screening.

 Laboratory analytical results indicate the presence of p-isopropyltoluene, PCE,
naphthalene, 1-methylnaphthalene, and 2-methylnaphthalene in one or more soil samples
collected adjacent to the trench drain at concentrations above the Soil-to-Water MSCCs.
The detected concentrations of these compounds do not exceed the Residential or
Industrial/Commercial MSCCs.

 Methylene chloride was also detected in samples SB-2 through SB-4; however,
methylene chloride is a common laboratory contaminant, particularly at the low
concentrations detected in soil samples collected at the Site. As such, the methylene
chloride detections are not likely representative of soil conditions at the Site.

 Results of the hypothetical worst-case risk calculations using soil data indicate that
cumulative carcinogenic and non-carcinogenic risks are below the DEQ and EPA
acceptable levels for residential and non-residential worker exposure scenarios.

 Groundwater analytical data do not indicate the presence of PAHs in groundwater at
concentrations above the respective 2L Standards. No VOCs were detected above the
laboratory method reporting limits in TMW-1 or TMW-2.

Phase II ESA soil and groundwater analytical data are summarized in Tables 1 and 2,
respectively.
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3.0 Receptor Information and Risk Characterization

As part of the Phase I LSA, H&H performed a Site land use and risk characterization survey.
The LSA Risk Classification and Land Use Form is provided in Appendix A. A discussion of
potential receptors and land use is provided below.

3.1 Receptor Information

3.1.1 Water Supply Wells

H&H conducted a water supply well survey for the area within a 1,000-ft radius of the source
area. The survey was conducted by performing area reconnaissance and checking for municipal
water connections. H&H also interviewed tenants and landowners of occupied properties within
500 ft of the source area regarding their water usage. As of the data of this report, two
completed Water Supply Well Information Survey forms were received by H&H and are
provided in Appendix B. Please note that based on information obtained during interviews with
nearby property owners during the survey, the properties within 500 ft of the source area are
connected to the municipal water supply and no water supply wells were identified.

Based on the water supply well survey, municipal water is available to all properties within a
1,000-ft radius of the Site and no water supply wells were identified.

3.1.2 Surface Water

H&H conducted a visual survey for surface water bodies in the area during the receptor survey.
Two unnamed tributaries of Cline Creek transect the southern portion of the Site. The closest
unnamed tributary of Cline Creek is located approximately 300 ft south of the source area (see
Figure 2).
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3.1.3 Subsurface Structures

Visual observations were made for potential subsurface contamination conduits in the immediate
vicinity of the service garage building. Based upon our review, there are no anticipated
subsurface contamination conduits of concern in the source area or nearby surrounding area.

3.1.4 Property Owners and Land Use

The Site is currently occupied by New South Tractor, a farm, construction, and lawn equipment
dealer. Surrounding properties are used primarily for commercial, manufacturing, and
residential purposes.

The Site is currently zoned Highway Business District (B-2) and General Manufacturing District
(M-1). The properties in the surrounding area are primarily zoned business (B-2 and B-4),
manufacturing (M-1), or residential (R-20A). The nearest residence is located approximately
350 ft northwest of the source area. Contiguous property owners are shown on Table 3 and
cross-referenced on Figure 3.

3.1.5 Wellhead Protection Areas

Based on our review of the DEQ Wellhead Protection Program’s (WHPP) SWAPInfo2.0
mapping database, the Site is not located in a wellhead protection area.

3.2 Risk and Land Use Characterization

Based upon the receptor data, as well as the Phase I LSA groundwater analytical data presented
in Section 5.0, the Site qualifies for a low-risk designation. In addition, based upon the zoning of
the Site and surrounding area, the Site qualifies for a commercial/industrial land use
classification.
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4.0 Geology and Hydrogeology

4.1 Regional Geology and Hydrogeology

The Site is in the Piedmont Physiographic Province of North Carolina. According to the
Geologic Map of North Carolina dated 1985, the subject property lies within the Inner Piedmont
Belt. In the Site area, underlying bedrock is composed of amphibolite and biotitic gneiss. The
land surface of the area is generally characterized as gently sloping, which may become
moderately steep where intersected by streams.

In the Piedmont, the bedrock is overlain by a mantle of weathered rock termed saprolite or
residuum. The saprolite consists of unconsolidated clay, silt, and sand with lesser amounts of
rock fragments. Due to the range of parent rock types and their variable susceptibility to
weathering, the saprolite ranges widely in color, texture, and thickness. Generally, the saprolite
is thickest near interstream divides and thins toward streambeds. In profile, the saprolite
normally grades from clayey soils near the land surface to highly weathered rock above
competent bedrock.

The occurrence and movement of groundwater in the Piedmont is typically within two separate
but interconnected water-bearing zones. A shallow water-bearing zone occurs within the
saprolite, and a deeper water-bearing zone occurs within the underlying bedrock.

4.2 Site Hydrogeology

Soil samples collected during the Phase I LSA indicate that soils in the source area consist
predominately of red, brown, and orange sandy clay and sandy silt to a depth of approximately
35 ft below ground surface (bgs).

Groundwater was encountered at a depth of approximately 27 ft bgs in temporary monitoring
well TMW-2A. Groundwater flow in the source area is expected to mimic topography and flow
primarily to the south towards two unnamed tributaries of Cline Creek.
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5.0 Soil and Groundwater Sampling

5.1 Soil and Groundwater Sampling Methodology

On March 6, 2023, H&H oversaw the advancement of LSA soil/boring temporary monitoring
well SB-3A/TMW-2A in the approximate former location of Phase II ESA boring/temporary
monitoring well SB-3/TMW-2 (see Figure 2).

Ameriprobe, LLC of Huntersville, North Carolina utilized a Geoprobe 7720 DT drill rig to
advance SB-3A/TMW-2A to approximately 35 ft bgs using direct push drilling methods. During
boring advancement, soil was recovered in 5 ft macrocore liners and evaluated for evidence of
impacts by visual observations, presence of odors, staining, and organic vapors as measured
using a calibrated photoionization detector (PID). A boring log including PID readings is
included in Appendix C.

DEQ UST Section guidelines indicate a soil sample should be collected every 5 ft when the
water table is less than 25 ft bgs. Although the depth to water of was measured at 26.72 ft bgs,
H&H conservatively collected four soil samples from boring SB-3A for laboratory analysis at
depth intervals of approximately 0-2 ft bgs, 7-9 ft bgs, 14-16 ft bgs, and 21-23 ft bgs. The soil
samples collected from 0-2 ft bgs and 21-23 ft bgs were analyzed for VOCs by EPA Method
8260D, SVOCs by EPA Method 8270E, VPH and EPH by Massachusetts Department of
Environmental Protection (MADEP) methods, and lead/chromium by EPA Method 6020B. The
two intermediate depth soil samples were submitted for laboratory analysis of VPH and EPH by
MADEP methods. Laboratory analyses were based on DEQ UST Section guidelines for a waste
oil release.

Temporary monitoring well TMW-2A was installed to a depth of approximately 35 ft bgs. The
well was constructed of 1-inch diameter PVC casing with a 15 ft section of 0.010-inch slot pre-
packed PVC screen that was set to bracket the water table. Filter sand was placed in the well
annulus from the base of the borehole to approximately 2 ft above the well screen, and a
hydrated bentonite seal was placed above the sand pack. On March 6, 2023, the depth to
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groundwater was measured at approximately 26.72 ft bgs using decontaminated electronic water
level indicator. A temporary well diagram is shown on the boring log provided in Appendix C.

Prior to groundwater sampling, H&H developed the temporary monitoring well using a
peristaltic pump and dedicated polyethylene tubing. The well was then purged using low-flow
methods, and H&H collected field measurements of temperature, pH, specific conductivity, and
oxidation reduction potential (ORP) during the purging process. A low-flow groundwater
sampling form is provided in Appendix D.

The groundwater sample from TMW-2A was submitted for laboratory analysis of VOCs by
Standard Method 6200B, SVOCs plus the 10 highest tentatively identified compounds (TICs) by
EPA Method 625, VPH and EPH by the MADEP Methods, and lead and chromium by EPA
Method 6020B.

The soil and groundwater samples were submitted to Pace Analytical, a North Carolina-certified
laboratory. Dedicated laboratory-supplied sample kits and bottles were used for sample
collection. The samples were placed in an iced cooler after collection. A chain-of-custody
record was completed for the samples collected and included the sample description, date
collected, time collected, matrix, sample container information, and analyses required. The
chain-of-custody was signed by field personnel prior to placement in the iced sample cooler for
shipment to the laboratory. The chain-of-custody record and laboratory analytical data sheets are
provided in Appendix E.

5.2 Soil Sampling Results

Soil analytical results for sample SB-3A (0-2) indicate the presence of several petroleum-related
VOCs, PAHs, C9-C18 aliphatics, and C9-C22 aromatics at concentrations above the Soil-to-
Groundwater MSCCs. The detection of total C9-C22 aromatics (820 mg/kg) also exceeds the
Residential MSCC of 469 mg/kg. Total chromium (75.5 mg/kg) and lead (12.7 mg/kg) were
detected at concentrations that are within the published ranges of background concentrations for
North Carolina soil of 7.0 to 300 mg/kg and non-detect to 50 mg/kg, respectively. Neither EPH
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nor VPH were detected above the laboratory method detection limits in the two intermediate
depth soil samples SB-3A (7-9) and SB-3A (14-16). Soil analytical results for the deeper sample
SB-3A (21-23) do not indicate the presence of VOCs, SVOCs, EPH, or VPH at concentrations
above the laboratory method detection limits. Lead and chromium were detected in soil sample
SB-3A (21-23) at concentrations consistent with published background levels for North Carolina
soil.

5.3 Groundwater Sampling Results

Groundwater analytical results for sample TMW-2A indicate the presence of several petroleum-
related VOCs, naphthalene, lead, and total chromium in TMW-2A at concentrations below the
2L Standards and GCLs. No aliphatics or aromatics were detected at concentrations above
laboratory detection limits.

5.4 Conclusion and Recommendations

Based on the results of the receptor survey and LSA soil and groundwater sampling, the Site
qualifies for a low-risk commercial/industrial classification.

Based upon the results of the Phase I LSA, H&H recommends that DEQ issue a risk-based NFA
letter for the release incident. As part of the NFA, H&H will complete public notice
requirements and file a NORP based on the presence of C9-C22 aromatics above the Residential
MSCC. Based on the isolated nature of soil contamination, H&H requests that an alternate
NORP restricting disturbance of impacted soil be approved to allow for future residential use of
the Site. A map showing the estimated extent of soil contamination will be attached to the
NORP.

Table 1Summary of Soil Analytical ResultsNew South Tractor977 and 985 US Highway 70Newton, North CarolinaH&H Job No. NST-001LocationNear Former Trench Drain Discharge PointSample ID SB-2 SB-3SB-4 SB-5Depth (ft bgs) 2-3 0-2 0-2 7-9 14-16 21-23 0-2 1-3Sample Date 9/15/2022 9/15/2022 9/15/2022 9/15/2022Assessment PhaseRange MeanUnitsVOCs (8260D)Acetone<0.206 <0.6460.0614 JNA NA <0.0513 <0.176 <0.13224 14,000 210,000-- --n-Butylbenzene<0.01030.446 0.774NA NA<0.0050 <0.0088 <0.00662.4 782 11,600-- --sec-Butylbenzene<0.01030.290 0.511NA NA<0.0035 <0.0088 <0.00662.2 1,560 23,300-- --Ethylbenzene<0.01030.0598 0.103NA NA<0.0037 <0.0088 <0.00668 60.3 297-- --p-Isopropyltoluene<0.01031.01 1.72NA NA<0.00390.012<0.00660.12 1,560 23,300-- --4-Methyl-2-pentanone<0.103 <0.3230.101NA NA<0.0077 <0.0881 <0.06590.42 1,250 18,600-- --Methylene Chloride0.445 0.499<0.0188NA NA<0.02190.327<0.02640.023 93.8 1,400-- --Naphthalene<0.01031.51 0.654NA NA<0.0042 <0.0088 <0.00660.2 5.5 27-- --n-Propylbenzene<0.01030.294 0.504NA NA<0.0028 <0.0088 <0.00661.4 1,560 23,300-- --Tetrachloroethylene<0.0103 <0.03230.0085NA NA<0.00250.0566<0.00660.005 93.8 1,400-- --Toluene<0.01030.0686 0.179NA NA<0.0055 <0.0088 <0.00665.4 1,250 18,600-- --1,2,4-Trimethylbenzene<0.01033.56 5.87NA NA<0.0047 <0.0088 <0.00666.6 156 2,330-- --1,3,5-Trimethylbenzene<0.01031.52 2.39NA NA<0.0027 <0.0088 <0.00666.6 156 2,330-- --m&p-Xylene<0.02060.248 0.475NA NA<0.0055 <0.0176 <0.013263,120 46,700----o-Xylene<0.01030.179 0.320NANA<0.0035 <0.0088 <0.006663,120 46,700----Xylenes, total<0.02060.427 0.795NANA<0.00460.0188<0.013263,120 46,700----EPH/VPH (MADEP)C5-C8 Aliphatics (VPH)NA NA <28.0 <14.0 <14.0 <13.0 NA NA68 625 9,340-- --C9-C12 Aliphatics (VPH)NA NA120<14.0 <14.0 <13.0 NA NANE NE NE-- --C9-C18 Aliphatics (EPH)NA NA840<12.0 <11.9 <12.6 NA NA540 1,560 23,300-- --Total C9-C18 Aliphatics NA NA960<26.0 <25.9 <25.6 NA NA540 1,560 23,300-- --C9-C10 Aromatics (VPH)NA NA130<14.0 <14.0 <13.0 NA NANE NE NE-- --C11-C22 Aromatics (EPH)NA NA690<12.0 <11.9 <12.6 NA NANE NE NE-- --Total C9-C22 Aromatics NA NA820<26.0 <25.9 <12.6 NANA314697,000----C19-C36 Aliphatics (EPH)NANA2,270<12.0 <11.9 <12.6 NANAImmobile 31,200 467,000----SVOCs/PAHs (8270E SIM)bis(2-Ethylexyl)phthalateNANA0.438NANA <0.162 NANA6.647233Fluorene<0.01180.174<0.142 NANA <0.1470.254 0.0135 556259,340----1-Methylnaphthalene<0.01180.883.46NANA <0.1471.190.0382 0.054 22.8112----2-Methylnaphthalene<0.01181.335.14NANA <0.1671.740.0462 1.562.5934----Naphthalene<0.01180.237 1.18NANA <0.1420.32<0.0120.25.527----Phenanthrene<0.01180.336 1.66NANA <0.1370.52 0.0311 644697,000----Metals (6020B)Chromium (Total)NA NA75.5NA NA21.7NA NA3.8 1.32 6.54 7.0 - 300 65LeadNA NA12.7NA NA13.8NA NA270 400 400 ND - 50 16Notes:1) DEQ Underground Storage Tank (UST) Section Maximum Soil Contaminant Concentrations (MSCCs) (September 2022).2) Range and mean values of background metals for North Carolina soils published in Elements in North American Soils by Dragun and Chekiri, 2005.Bold values exceed the Soil-to-Water MSCC.Underlined value exceeds the Residential MSCC.Soil concentrations are reported in milligrams per kilogram (mg/kg).VOCs = volatile organic compounds; PAH = polycyclic aromatic hydrocarbons; SVOCs = semi-VOCs; EPH = extractable petroleum hydrocarbons; VPH = volatile petroleum hydrocarbons;MADEP = Massachusetts Department of Environmental Protection; ft bgs = feet below ground surface; NA = not analyzed; NE = not established; -- = not applicable; UST = underground storage tank; LSA = Limited Site AssessmentJ = estimated concentration that is above the laboratory method detection limit but below the laboratory reporting limit; SIM = Selected Ion MonitoringLaboratory analytical methods are shown in parentheses.ft bgs = feet below ground surfaceOnly analytes detected in at least one sample shown.mg/kgPublished Background Metals Concentrations for North Carolina Soils (2)Due DiligenceScreening CriteriaTrench DrainSoil-to-Water MSCCs(1)Residential MSCCs(1)Industrial/ Commercial MSCCs(1)SB-3A3/6/2023LSADue Diligencehttps://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/New South Tractor/LSA/Tables/NST.001 - LSA Tables 1 and 23/30/2023Table 1 (Page 1 of 1)Hart & Hickman, PC
Table 2
Summary of Groundwater Analytical Data
New South Tractor
977 and 985 US Highway 70
Newton, North Carolina
H&H Job No. NST-001
Location Description South of Southern
Building
Sample ID TMW-1 TMW-2 TMW-2A
Date 9/15/2022 9/15/2022 3/6/2023
Assessment Phase LSA
Units
VOCs (8260D/6200B)
Naphthalene <1.0 <1.0 1.5 J 6 6,000
1,2,4-Trimethylbenzene NA NA 1.7 400 28,500
1,3,5-Trimethylbenzene NA NA 0.72 400 24,100
SVOCs/PAHs (625/8270E)
1-Methylnaphthalene <0.80 0.89 NA 1 1,000
2-Methylnaphthalene <0.80 0.90 NA 30 12,000
Naphthalene <1.5 <1.5 3.2 J 6 6,000
Tentatively Identified Compounds (TICs)
Ethylbenzene NA NA 13.7 J 600 80,000
p-Xylene NA NA 44.1 J 500 50,000
p-Xylene NA NA 20.7 J 500 50,000
Benzene, 1-ethy-3methyl NA NA 11.6 J NE NE
n-Hexadecanoic acid NA NA 5.8 J NE NE
Toluene NA NA 78.8 J 600 260,000
Unknown NA NA 10.6 J NE NE
Unknown NA NA 8.4 J NE NE
VPH/EPH (MADEP)
C5-C8 Aliphatics (VPH)NA NA <100 400 NE
C9-C12 Aliphatics (VPH)NA NA <100 NE NE
C9-C18 Aliphatics (EPH)NA NA <97.1 700 NE
Total C9-C18 Aliphatics NA NA <197.1 700 NE
C9-C10 Aromatics (VPH)NA NA <100 NE NE
C11-C22 Aromatics (EPH)NA NA <97.1 NE NE
Total C9-C22 Aromatics NA NA <197.1 200 NE
C19-C36 Aliphatics (EPH)NA NA <97.1 10,000 NE
Metals (6020B)
Chromium NA NA 0.60 J 10 10,000
Lead NA NA 0.32 J 15 15,000
Notes:
1) North Carolina Department of Environmental Quality (DEQ) 15A NCAC 02L.0202 Groundwater Standards (2L Standards), dated April 2022.
2) DEQ UST Section Gross Contamination Levels (GCLs) dated October 2020.
Concentrations are reported in micrograms per liter (µg/L).
VOCs = volatile organic compounds; PAHs = polynuclear aromatic hydrocarbons; SVOCs = semi-VOCs; EPH = extractable petroleum hydrocarbons
VPH = Volatile Petroleum Hydrocarbons;
NA = not analyzed; NE = not established
Only analytes detected in at least one sample shown.
Method number follows analysis in parenthesis.
J = Estimated concentration above the laboratory method detection limit and below the laboratory reporting limit.
µg/L
Due Diligence
Gross
Contamination
Levels (2)
Trench Drain
NC 2L Groundwater
Standards(1)
Screening Criteria
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/New South Tractor/LSA/Tables/NST.001 - LSA Tables 1 and 2
3/30/2023
Table 2 (Page 1 of 1)
Hart & Hickman, PC
Table 3Summary of Contiguous PropertiesNew South Tractor977 and 985 US Highway 70Newton North CarolinaH&H Job. No. NST-001373110458022 A 973 US Highway 70East373114446744 B Unspecified AddressEast373114446401 C 2968 Hughey Dr.Covenant Christian Church of Catawba County, Inc.PO Box 731Conover, NC 28613Southeast373114444503 D 2971 Hughey Dr.South373114442557 E 1005 Pine St.South373114440872 F Unspecified AddressWest373110451332 G 1061 US Highway 70West373110359772 H 1022 Conover Blvd. West John Glen McCall II1655 Beverly St.Newton, NC 28658Northwest373110451746 I 1016 Conover Blvd. West Ker Thao and Mee K. Thao1016 Conover Blvd. West Conover, NC 28613Northwest373110452642 J 1006 Conover Blvd. West James Gregory Burgess1273 Murrays Mill Rd. Catawba, NC 28609North373110453691 K 1002 Conover Blvd. WestNathan Scott Rhodes and Marcie R. RuftiePO Box 687 Conover, NC 28613North373110456646 L 924 Conover Blvd. West Bakatsias Rental Properties, LLC924 Conover Blvd. WestConover, NC 28613North373110458686 M 920 Conover Blvd. West Andrew T. DeHart and Bridget C. DeHartPO Box 330023Atlantic Beach, FL 32233NortheastNotes:Property owner information is based on the Catawba County GIS website.Contiguous properties are shown on Figure 3.F&E Properties, LLC1421 Sugar Farm Rd.Catawba, NC 28609Jose Luis Garcia Montano11209 Johnson Davis Rd.Huntersville, NC 28078Commercial Signs Outdoor, Inc.133 S Main StGranite Falls, NC 28630Parcel ID No. Map ID Property Street Address Owner Owner AddressDirection From Site https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/New South Tractor/LSA/Tables/Table 3 - Adjacent Properties3/30/2023Table 3 (Page 1 of 1)Hart & Hickman, PC
USGS The National Map: National Boundaries Dataset, 3DEP ElevationProgram, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset,and National Transportation Dataset; USGS Global Ecosystems; U.S.Census Bureau TIGER/Line data; USFS Road Data; Natural Earth Data;U.S. Department of State Humanitarian Information Unit; and NOAANational Centers for Environmental Information, U.S. Coastal ReliefModel. Data refreshed June, 2022.
SITE LOCATION MAP
NEW SOUTH TRACTOR977 AND 985 US HIGHWAY 70NEWTON, NORTH CAROLINA
DATE: 3-20-22
JOB NO: NST-001
REVISION NO: 0
FIGURE NO: 1
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
TITLE
PROJECT
0 2,000 4,000
SCALE IN FEET
SITE
Path: S:\AAA-Master Projects\New South Tractor\Phase II\Figures\Figure-1.mxdN
U.S.G.S. QUADRANGLE MAP
NEWTON, NORTH CAROLINA 2019
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)
REVISION NO. 0
JOB NO. NST-001
DATE: 3-20-23
FIGURE NO. 2
NEW SOUTH TRACTOR
977 AND 985 US HIGHWAY 70
NEWTON, NORTH CAROLINA
SITE AND SAMPLE LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL LINE
SURFACE WATER FEATURE
POLE-MOUNTED TRANSFORMER
SEPTIC SYSTEM
TRENCH DRAIN
DUMPSTER
SOIL BORING LOCATION
CO-LOCATED SOIL BORING AND
TEMPORARY MONITORING WELL
NOTES:
1. AERIAL IMAGERY OBTAINED FROM NC ONEMAP, 2018.
2. BASE DATA OBTAINED FROM CATAWBA COUNTY GIS,
2019.
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
CONOVER BOULEVARD WEST
HUGHEY DRIVEPIN
E

S
T
R
E
E
TFREEMAN AVENUEBP TIRE & SERVICE
(973 US-70 W.)
BENNETT BUILDING OF CONOVER
(920 CONOVER BOULEVARD W.)
TRADING POST OF CONOVER
(102 CONOVER BOULEVARD W.)PALERMO'S FAMILY ITALIAN
& GREEK RESTAURANT
(924 CONOVER BOULEVARD W.)UNDEVELOPEDUNDEVELOPED
COVENANT CHRISTIAN CHURCH
(2968 HUGHEY DRIVE)
ABANDONED BOX TRUCK
ABANDONED CAR
RESIDENCE
(1016 CONOVER BOULEVARD W.)
UDDERLY DELICIOUS ICE CREAM
(1006 CONOVER BOULEVARD W.)
(2) ROLL OFF DUMPSTERS
DEBRIS OBSERVED
(1) AIR COMPRESSOR
(1) 300-GALLON DIESEL AST
WASTE OIL HEATER
OFFICE/SALES/STOREFRONT AREA
SERVICE DEPARTMENT
NEW AND USED OIL
275-GALLON STORAGE TOTES
AIR COMPRESSOR
55-GALLON DRUMS
OF METHANOL
SHED
55-GALLON USED
OIL DRUMS
SB-2
SB-3/TMW-2
SB-1/TMW-1
SB-4
SB-5
SB-3A/TMW-2A
S:\AAA-Master Projects\New South Tractor\LSA\Figures\NST-001 LSA.dwg, FIG 2, 3/20/2023 5:35:20 PM, sperry
REVISION NO. 0
JOB NO. NST-001
DATE: 3-20-23
FIGURE NO. 3
NEW SOUTH TRACTOR
977 AND 985 US HIGHWAY 70
NEWTON, NORTH CAROLINA
CONTIGUOUS PROPERTIES AND
RECEPTOR SURVEY MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL LINE
SURFACE WATER FEATURE
CONTIGUOUS PROPERTY ID
(SEE TABLE 3)
NOTES:
1.AERIAL IMAGERY OBTAINED FROM NC ONEMAP, 2018.
2.BASE DATA OBTAINED FROM CATAWBA COUNTY GIS,
2019.
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
CONOVER BOULEVARD WEST
HUGHEY DRIVEFREEMAN AVENUE250 FT
500 FT
1,000 FT
S:\AAA-Master Projects\New South Tractor\LSA\Figures\NST-001 LSA.dwg, FIG 3, 3/20/2023 6:22:10 PM, sperry

Appendix A

Risk Classification and Land Use Form
1
Limited Site Assessment Risk Classification and Land Use Form

Part I - Groundwater/Surface Water/Vapor Impacts
High Risk

1. Has the discharge or release contaminated any water supply well including any used
for non-drinking purposes?

The discharge or release has not resulted in known contaminated water wells in the site
area.

2. Is a water supply well used for drinking water located within 1,000 feet of the source
area of the discharge or release?

Water supply wells used for drinking water were not identified within 1,000 ft of the
source area.

3. Is a water supply well used for any purpose (e.g., irrigation, washing cars, industrial
cooling water, filling swimming pools) located within 250 feet of the source area of the
release or discharge?

Water supply wells used for any purpose were not identified within 250 ft of the source
area.

4. Does groundwater within 500 feet of the source area of the discharge or release have
the potential for future use in that there is no other source of water supply other than the
groundwater?

The subject site and surrounding properties are served by the municipal water supply.

5. Do vapors from the discharge or release pose a threat of explosion because of
accumulation of the vapors in a confined space, or pose any other serious threat to public
health, public safety or the environment?

Vapors from the discharge or release do not pose a threat of explosion and do not pose a
serious threat to public health, public safety, or the environment.

6. Are there any other factors that would cause the discharge or release to pose an
imminent danger to public health, public safety, or the environment?

No other factors would cause the discharge or release to pose an imminent danger to
public health, public safety, or the environment.
2
Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the discharge or
release?
According to the USGS topographic map, an unnamed tributary of Cline Creek is located
approximately 300 feet south of the source area.
8. Is the source area of the discharge or release located within a designated wellhead
protection area as defined in 42 USC 300h-7(e)?
The source area is not located within a designated wellhead protection area.
9. Is the discharge or release located in the Coastal Plain physiographic region as
designated on a map entitled "Geology of North Carolina" published by the Department
in 1985? If yes, is the source area of the discharge or release located in an area in which
there is recharge to an unconfined or semi-confined deeper aquifer that is being used or
may be used as a source of drinking water?
The discharge or release is not located in the Coastal Plain physiographic region.
10. Do the levels of groundwater contamination for any contaminant exceed the gross
contamination levels established (see Table 3) by the Department?
Detected concentrations do not exceed Gross Contamination Levels.
Part II - Land Use
Property Containing Source Area of Discharge or Release
1. Does the property contain one or more primary or secondary residences (permanent or
temporary)?
The property does not contain a primary or secondary residence.
2. Does the property contain a school, daycare center, hospital, playground, park,
recreation area, church, nursing home, or other place of public assembly?
The property does not contain a place of public assembly.
3. Does the property contain a commercial (e.g., retail, warehouse, office/business space,
etc.) or industrial (e.g., manufacturing, utilities, industrial research and development,
chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial
enterprise, or is the land undeveloped?
The property is currently developed with an approximately 11,600-square foot (sq ft)
industrial office/service garage building that was constructed in 1962 and a roughly
3
4,800-sq ft storage/garage building that was constructed in the early to mid-1960s. The
Site is occupied by New South Tractor, a farm, construction, and lawn equipment dealer.
The remainder of the site consists of paved parking areas and driveways, concrete
loading and storage areas, gravel storage areas, and undeveloped land.
4. Do children visit the property?
Children currently do not visit the property.
5. Is access to the property reliably restricted consistent with its use (e.g., by fences,
security personnel or both)?
Access to the property is currently restricted by a fence.
6. Do pavement, buildings, or other structures cap the contaminated soil?
The area of the trench drain release is capped with a concrete slab foundation..
7. What is the zoning status of the property?
The property is zoned Highway Business District (B-2) and General Manufacturing District (M-1).
8. Is the use of the property likely to change in the next 20 years?
The use will not likely change in the next 20 years.
Property Surrounding Source Area of Discharge or Release
The questions below pertain to the area within 1500 feet of the source area of the discharge or
release (excludes property containing source area of the release):
9. What is the distance from the source area of the release to the nearest primary or
secondary residence (permanent or temporary)?
The nearest residence is located approximately 350 ft northwest of the source area.
10. What is the distance from the source area of the release to the nearest school, daycare
center, hospital, playground, park, recreation area, church, nursing home or other place of
public assembly?
Covenant Christian Church is located approximately 800 ft southeast of the source area.
4
11. What is the zoning status of properties in the surrounding area?
The properties in the surrounding area are primarily zoned business (B-2, B-4),
manufacturing (M-1), or residential (R-20A).
12. Briefly characterize the use and activities of the land in the surrounding area.
The primary land use in the immediate vicinity of the site is commercial, residential, and
light industrial.

Appendix B

Water Supply Well Information Survey Forms

Appendix C

Boring Log
NOTES: Boring hand augered to 5' bgs to clear subsurface utilities.
generated using GroundLogs.online
Client:
Project:
Address:
New South Tractor
NST-001
977 & 985 US Hwy 70, Newton, NC
WELL LOG
Well No.
Page:
TMW-2A/SB-3A
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/6/2023
3/6/2023
Ameriprobe
Direct Push
Geoprobe 7720DT
John Allen
Derek Haskell
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
35.0
3.25
DP, GR
26.72
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
35.0
1.0
0.010
Sch 40 PVC
PVC Prepack
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
35
40
GR
DP
DP
DP
DP
DP
DP
5.00
5.00
5.00
5.00
5.00
5.00
5.00
(0') Concrete
(0.75') Sandy lean CLAY (CL); medium plasticity, medium stiff, moist, red-brown
(7') Sandy lean CLAY (CL); medium plasticity, medium stiff, moist, red-brown and
light brown, micaceous
(11') Sandy SILT (ML); medium stiff, moist, light brown and red-brown, micaceous
(16') SILT (ML); few fine-coarse sand, medium stiff, moist, black and orange-brown,
micaceous
(17') Sandy SILT (ML); medium stiff, moist, tan/red-brown/gray/white, saprolite,
micaceous
(26') Sandy SILT (ML); medium stiff, wet, orange/black/white/tan, saprolite,
micaceous
(30') Sandy SILT (ML); soft, saturated, brown/orange/white/gray, saprolite,
micaceous
(35') Boring terminated
176.4
83.4
49.9
2.3
2.4
1.5
1.6
1.0
0.4
0.6
0.2
1.2
1.6
SB-3A(0-2)
0
5
10
15
20
25
30
35
40
SB-3A(7-9)
SB-3A(21-23)
SB-3A(14-16)

Appendix D

Low-Flow Groundwater Sampling Form
6?%%%0DVWHU7HPSODWHV?)RUPV)RUPV?/RZ)ORZ*URXQGZDWHU6DPSOLQJ)RUPSGI/DVW8SGDWHGJob No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________Depth to Water (ft :___________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIW BBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ftWeather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6&RQG253P9'2PJ/NST.001New South TractorNewton, NC3/6/2334.75DJH3370s F, sunnystart@1235; stickup=0.1'DO cable was broken on YSI-002, unable toget accurate DO readings duringpurging12:4012:4512:5012:5527.2627.3127.3627.361L2L3L4L200 mL/min200 mL/min200 mL/min200 mL/min19.919.919.819.8173.8176.0178.7178.16.025.975.975.9794.392.4104.7105.513.0023.0014.208.17n/aYSI-002, HACH-003DJH 3/6/2023x4 40 mL VOAs(VOCs 6200)w/ HCL;x3 40 mL VOAs(VPH MADEP)w/ HCL; x2 100 mL ambers(SVOA 625+TICs)unpres.; x1 250 mLplastic(lead/chromium 6020)w/ HNO3;x2 1 L ambers(EPH MADEP)w/ HCLPeristalticPVC1-inch12:55Pace AnalyticalTMW-2A2035PolyethyleneTOC26.720.34TOCTOCgallons

Appendix E

Laboratory Analytical Report
#=CL#
March 15, 2023
LIMS USE: FR - BO CAPPLEMAN
LIMS OBJECT ID: 92655319
92655319
Project:
Pace Project No.:
RE:
Bo Cappleman
Hart & Hickman
2923 South Tryon Street
Charlotte, NC 28203
NST .001-002
Dear Bo Cappleman:
Enclosed are the analytical results for sample(s) received by the laboratory on March 06, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Minneapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 83
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92655319
NST .001-002
Pace Analytical Services, LLC - Minneapolis MN
1700 Elm Street SE, Minneapolis, MN 55414
A2LA Certification #: 2926.01*
1800 Elm Street SE, Minneapolis, MN 55414--Satellite Air
Lab
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009*
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014*
Arkansas DW Certification #: MN00064
Arkansas WW Certification #: 88-0680
California Certification #: 2929
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8 Tribal Water Systems+Wyoming DW
Certification #: via MN 027-053-137
Florida Certification #: E87605*
Georgia Certification #: 959
GMP+ Certification #: GMP050884
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: AI-03086*
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064*
Maryland Certification #: 322
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137*
Minnesota Dept of Ag Approval: via MN 027-053-137
Minnesota Petrofund Registration #: 1240*
Mississippi Certification #: MN00064
Missouri Certification #: 10100
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081*
New Jersey Certification #: MN002
New York Certification #: 11647*
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification (A2LA) #: R-036
North Dakota Certification (MN) #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification (1700) #: CL101
Ohio VAP Certification (1800) #: CL110*
Oklahoma Certification #: 9507*
Oregon Primary Certification #: MN300001
Oregon Secondary Certification #: MN200001*
Pennsylvania Certification #: 68-00563
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192*
Utah Certification #: MN00064*
Vermont Certification #: VT-027053137
Virginia Certification #: 460163*
Washington Certification #: C486*
West Virginia DEP Certification #: 382
West Virginia DW Certification #: 9952 C
Wisconsin Certification #: 999407970
Wyoming UST Certification #: via A2LA 2926.01
USDA Permit #: P330-19-00208
*Please Note: Applicable air certifications are denoted with
an asterisk (*).
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 83
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92655319
NST .001-002
Lab ID Sample ID Matrix Date Collected Date Received
92655319001 SB-3A (0-2)Solid 03/06/23 13:45 03/06/23 15:45
92655319002 SB-3A (7-9)Solid 03/06/23 13:55 03/06/23 15:45
92655319003 SB-3A (14-16)Solid 03/06/23 14:05 03/06/23 15:45
92655319004 SB-3A (21-23)Solid 03/06/23 14:15 03/06/23 15:45
92655319005 TMW-2A Water 03/06/23 12:55 03/06/23 15:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 83
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92655319
NST .001-002
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92655319001 SB-3A (0-2)MADEP EPH 7 PASI-CBAJ
EPA 6020B 2 PASI-MNN2
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92655319002 SB-3A (7-9)MADEP EPH 7 PASI-CBAJ
SW-846 1 PASI-CKDF
92655319003 SB-3A (14-16)MADEP EPH 7 PASI-CBAJ
SW-846 1 PASI-CKDF
92655319004 SB-3A (21-23)MADEP EPH 7 PASI-CBAJ
EPA 6020B 2 PASI-MNN2
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92655319005 TMW-2A MADEP EPH 7 PASI-CBAJ
EPA 6020B 2 PASI-AKRL
EPA 625.1 66 PASI-CPKS
SM 6200B 63 PASI-CLMB
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-M = Pace Analytical Services - Minneapolis
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655319
NST .001-002
Sample:SB-3A (0-2)Lab ID:92655319001 Collected:03/06/23 13:45 Received:03/06/23 15:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)840 mg/kg 03/10/23 17:24 N203/07/23 14:5962162150
Aliphatic (C19-C36)2270 mg/kg 03/10/23 17:24 N203/07/23 14:5962162150
Aromatic (C11-C22)690 mg/kg 03/10/23 17:24 N203/07/23 14:5949.7 49.7 4
Surrogates
1-Chlorooctadecane (S)0 %03/10/23 17:24 3386-33-2 S403/07/23 14:5940-140 50
o-Terphenyl (S)367 %03/10/23 17:24 84-15-1 S503/07/23 14:5940-140 4
2-Fluorobiphenyl (S)121 %03/10/23 17:24 321-60-803/07/23 14:5940-140 4
2-Bromonaphthalene (S)429 %03/10/23 17:24 580-13-2 S503/07/23 14:5940-140 4
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Chromium 75.5 mg/kg 03/09/23 17:14 7440-47-3 M1,R103/09/23 10:342.4 0.47 1
Lead 12.7 mg/kg 03/09/23 17:14 7439-92-103/09/23 10:340.61 0.11 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 03/08/23 15:51 83-32-903/07/23 09:434041421
Acenaphthylene ND ug/kg 03/08/23 15:51 208-96-803/07/23 09:434041421
Aniline ND ug/kg 03/08/23 15:51 62-53-303/07/23 09:434041581
Anthracene ND ug/kg 03/08/23 15:51 120-12-703/07/23 09:434041321
Benzo(a)anthracene ND ug/kg 03/08/23 15:51 56-55-303/07/23 09:434041351
Benzo(a)pyrene ND ug/kg 03/08/23 15:51 50-32-803/07/23 09:434041401
Benzo(b)fluoranthene ND ug/kg 03/08/23 15:51 205-99-203/07/23 09:434041351
Benzo(g,h,i)perylene ND ug/kg 03/08/23 15:51 191-24-203/07/23 09:434041571
Benzo(k)fluoranthene ND ug/kg 03/08/23 15:51 207-08-903/07/23 09:434041421
Benzoic Acid ND ug/kg 03/08/23 15:51 65-85-003/07/23 09:4320208691
Benzyl alcohol ND ug/kg 03/08/23 15:51 100-51-603/07/23 09:438083061
4-Bromophenylphenyl ether ND ug/kg 03/08/23 15:51 101-55-303/07/23 09:434041561
Butylbenzylphthalate ND ug/kg 03/08/23 15:51 85-68-703/07/23 09:434041701
4-Chloro-3-methylphenol ND ug/kg 03/08/23 15:51 59-50-703/07/23 09:438082841
4-Chloroaniline ND ug/kg 03/08/23 15:51 106-47-803/07/23 09:438083171
bis(2-Chloroethoxy)methane ND ug/kg 03/08/23 15:51 111-91-103/07/23 09:434041681
bis(2-Chloroethyl) ether ND ug/kg 03/08/23 15:51 111-44-403/07/23 09:434041521
2-Chloronaphthalene ND ug/kg 03/08/23 15:51 91-58-703/07/23 09:434041601
2-Chlorophenol ND ug/kg 03/08/23 15:51 95-57-803/07/23 09:434041521
4-Chlorophenylphenyl ether ND ug/kg 03/08/23 15:51 7005-72-303/07/23 09:434041511
Chrysene ND ug/kg 03/08/23 15:51 218-01-903/07/23 09:434041471
Dibenz(a,h)anthracene ND ug/kg 03/08/23 15:51 53-70-303/07/23 09:434041561
Dibenzofuran ND ug/kg 03/08/23 15:51 132-64-903/07/23 09:434041461
1,2-Dichlorobenzene ND ug/kg 03/08/23 15:51 95-50-103/07/23 09:434041461
1,3-Dichlorobenzene ND ug/kg 03/08/23 15:51 541-73-103/07/23 09:434041431
1,4-Dichlorobenzene ND ug/kg 03/08/23 15:51 106-46-703/07/23 09:434041541
3,3'-Dichlorobenzidine ND ug/kg 03/08/23 15:51 91-94-103/07/23 09:438082731
2,4-Dichlorophenol ND ug/kg 03/08/23 15:51 120-83-203/07/23 09:434041581
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655319
NST .001-002
Sample:SB-3A (0-2)Lab ID:92655319001 Collected:03/06/23 13:45 Received:03/06/23 15:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Diethylphthalate ND ug/kg 03/08/23 15:51 84-66-203/07/23 09:434041481
2,4-Dimethylphenol ND ug/kg 03/08/23 15:51 105-67-903/07/23 09:434041681
Dimethylphthalate ND ug/kg 03/08/23 15:51 131-11-303/07/23 09:434041471
Di-n-butylphthalate ND ug/kg 03/08/23 15:51 84-74-203/07/23 09:434041361
4,6-Dinitro-2-methylphenol ND ug/kg 03/08/23 15:51 534-52-1 v103/07/23 09:438083771
2,4-Dinitrophenol ND ug/kg 03/08/23 15:51 51-28-5 v103/07/23 09:43202012501
2,4-Dinitrotoluene ND ug/kg 03/08/23 15:51 121-14-203/07/23 09:434041561
2,6-Dinitrotoluene ND ug/kg 03/08/23 15:51 606-20-203/07/23 09:434041481
Di-n-octylphthalate ND ug/kg 03/08/23 15:51 117-84-003/07/23 09:434041591
bis(2-Ethylhexyl)phthalate 438 ug/kg 03/08/23 15:51 117-81-703/07/23 09:434041571
Fluoranthene ND ug/kg 03/08/23 15:51 206-44-003/07/23 09:434041381
Fluorene ND ug/kg 03/08/23 15:51 86-73-703/07/23 09:434041421
Hexachloro-1,3-butadiene ND ug/kg 03/08/23 15:51 87-68-303/07/23 09:434041751
Hexachlorobenzene ND ug/kg 03/08/23 15:51 118-74-103/07/23 09:434041581
Hexachlorocyclopentadiene ND ug/kg 03/08/23 15:51 77-47-403/07/23 09:434042321
Hexachloroethane ND ug/kg 03/08/23 15:51 67-72-103/07/23 09:434041541
Indeno(1,2,3-cd)pyrene ND ug/kg 03/08/23 15:51 193-39-503/07/23 09:434041591
Isophorone ND ug/kg 03/08/23 15:51 78-59-103/07/23 09:434041801
1-Methylnaphthalene 3460 ug/kg 03/08/23 15:51 90-12-003/07/23 09:434041421
2-Methylnaphthalene 5140 ug/kg 03/09/23 18:00 91-57-603/07/23 09:438083232
2-Methylphenol(o-Cresol)ND ug/kg 03/08/23 15:51 95-48-703/07/23 09:434041651
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/08/23 15:51 15831-10-403/07/23 09:434041631
Naphthalene 1180 ug/kg 03/08/23 15:51 91-20-303/07/23 09:434041371
2-Nitroaniline ND ug/kg 03/08/23 15:51 88-74-403/07/23 09:4320203311
3-Nitroaniline ND ug/kg 03/08/23 15:51 99-09-203/07/23 09:4320203171
4-Nitroaniline ND ug/kg 03/08/23 15:51 100-01-603/07/23 09:438083071
Nitrobenzene ND ug/kg 03/08/23 15:51 98-95-303/07/23 09:434041871
2-Nitrophenol ND ug/kg 03/08/23 15:51 88-75-503/07/23 09:434041751
4-Nitrophenol ND ug/kg 03/08/23 15:51 100-02-703/07/23 09:4320207821
N-Nitrosodimethylamine ND ug/kg 03/08/23 15:51 62-75-903/07/23 09:434041361
N-Nitroso-di-n-propylamine ND ug/kg 03/08/23 15:51 621-64-703/07/23 09:434041521
N-Nitrosodiphenylamine ND ug/kg 03/08/23 15:51 86-30-603/07/23 09:434041431
2,2'-Oxybis(1-chloropropane)ND ug/kg 03/08/23 15:51 108-60-103/07/23 09:434041921
Pentachlorophenol ND ug/kg 03/08/23 15:51 87-86-503/07/23 09:438083961
Phenanthrene 1660 ug/kg 03/08/23 15:51 85-01-803/07/23 09:434041321
Phenol ND ug/kg 03/08/23 15:51 108-95-203/07/23 09:434041801
Pyrene ND ug/kg 03/08/23 15:51 129-00-003/07/23 09:434041641
Pyridine ND ug/kg 03/08/23 15:51 110-86-103/07/23 09:434041271
1,2,4-Trichlorobenzene ND ug/kg 03/08/23 15:51 120-82-103/07/23 09:434041591
2,4,5-Trichlorophenol ND ug/kg 03/08/23 15:51 95-95-403/07/23 09:434041851
2,4,6-Trichlorophenol ND ug/kg 03/08/23 15:51 88-06-203/07/23 09:434041671
Surrogates
Nitrobenzene-d5 (S)70 %03/08/23 15:51 4165-60-003/07/23 09:4310-130 1
2-Fluorobiphenyl (S)68 %03/08/23 15:51 321-60-803/07/23 09:4310-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655319
NST .001-002
Sample:SB-3A (0-2)Lab ID:92655319001 Collected:03/06/23 13:45 Received:03/06/23 15:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Terphenyl-d14 (S)60 %03/08/23 15:51 1718-51-003/07/23 09:4310-130 1
Phenol-d6 (S)62 %03/08/23 15:51 13127-88-303/07/23 09:4310-130 1
2-Fluorophenol (S)64 %03/08/23 15:51 367-12-403/07/23 09:4310-130 1
2,4,6-Tribromophenol (S)71 %03/08/23 15:51 118-79-603/07/23 09:4310-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 61.4J ug/kg 03/07/23 00:07 67-64-103/06/23 20:3813744.1 1
Benzene ND ug/kg 03/07/23 00:07 71-43-203/06/23 20:386.9 2.7 1
Bromobenzene ND ug/kg 03/07/23 00:07 108-86-103/06/23 20:386.9 2.2 1
Bromochloromethane ND ug/kg 03/07/23 00:07 74-97-503/06/23 20:386.9 2.0 1
Bromodichloromethane ND ug/kg 03/07/23 00:07 75-27-403/06/23 20:386.9 2.6 1
Bromoform ND ug/kg 03/07/23 00:07 75-25-203/06/23 20:386.9 2.4 1
Bromomethane ND ug/kg 03/07/23 00:07 74-83-903/06/23 20:3827.4 21.3 1
2-Butanone (MEK)ND ug/kg 03/07/23 00:07 78-93-303/06/23 20:3813732.9 1
n-Butylbenzene 774 ug/kg 03/07/23 00:07 104-51-803/06/23 20:386.9 4.3 1
sec-Butylbenzene 511 ug/kg 03/07/23 00:07 135-98-803/06/23 20:386.9 3.0 1
tert-Butylbenzene ND ug/kg 03/07/23 00:07 98-06-603/06/23 20:386.9 2.4 1
Carbon tetrachloride ND ug/kg 03/07/23 00:07 56-23-5 IK03/06/23 20:386.9 2.6 1
Chlorobenzene ND ug/kg 03/07/23 00:07 108-90-703/06/23 20:386.9 3.9 1
Chloroethane ND ug/kg 03/07/23 00:07 75-00-303/06/23 20:3813.7 5.3 1
Chloroform ND ug/kg 03/07/23 00:07 67-66-303/06/23 20:386.9 5.7 1
Chloromethane ND ug/kg 03/07/23 00:07 74-87-303/06/23 20:3813.7 5.8 1
2-Chlorotoluene ND ug/kg 03/07/23 00:07 95-49-803/06/23 20:386.9 2.4 1
4-Chlorotoluene ND ug/kg 03/07/23 00:07 106-43-403/06/23 20:386.9 3.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/07/23 00:07 96-12-803/06/23 20:386.9 2.7 1
Dibromochloromethane ND ug/kg 03/07/23 00:07 124-48-1 IK03/06/23 20:386.9 3.9 1
1,2-Dibromoethane (EDB)ND ug/kg 03/07/23 00:07 106-93-403/06/23 20:386.9 3.0 1
Dibromomethane ND ug/kg 03/07/23 00:07 74-95-303/06/23 20:386.9 1.5 1
1,2-Dichlorobenzene ND ug/kg 03/07/23 00:07 95-50-103/06/23 20:386.9 2.5 1
1,3-Dichlorobenzene ND ug/kg 03/07/23 00:07 541-73-103/06/23 20:386.9 2.1 1
1,4-Dichlorobenzene ND ug/kg 03/07/23 00:07 106-46-703/06/23 20:386.9 1.8 1
Dichlorodifluoromethane ND ug/kg 03/07/23 00:07 75-71-803/06/23 20:3813.7 7.0 1
1,1-Dichloroethane ND ug/kg 03/07/23 00:07 75-34-303/06/23 20:386.9 2.8 1
1,2-Dichloroethane ND ug/kg 03/07/23 00:07 107-06-203/06/23 20:386.9 4.5 1
1,1-Dichloroethene ND ug/kg 03/07/23 00:07 75-35-403/06/23 20:386.9 2.8 1
cis-1,2-Dichloroethene ND ug/kg 03/07/23 00:07 156-59-203/06/23 20:386.9 2.3 1
trans-1,2-Dichloroethene ND ug/kg 03/07/23 00:07 156-60-503/06/23 20:386.9 5.8 1
1,2-Dichloropropane ND ug/kg 03/07/23 00:07 78-87-503/06/23 20:386.9 2.1 1
1,3-Dichloropropane ND ug/kg 03/07/23 00:07 142-28-903/06/23 20:386.9 2.1 1
2,2-Dichloropropane ND ug/kg 03/07/23 00:07 594-20-703/06/23 20:386.9 5.2 1
1,1-Dichloropropene ND ug/kg 03/07/23 00:07 563-58-6 v103/06/23 20:386.9 3.3 1
cis-1,3-Dichloropropene ND ug/kg 03/07/23 00:07 10061-01-503/06/23 20:386.9 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655319
NST .001-002
Sample:SB-3A (0-2)Lab ID:92655319001 Collected:03/06/23 13:45 Received:03/06/23 15:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
trans-1,3-Dichloropropene ND ug/kg 03/07/23 00:07 10061-02-603/06/23 20:386.9 2.4 1
Diisopropyl ether ND ug/kg 03/07/23 00:07 108-20-303/06/23 20:386.9 1.9 1
Ethylbenzene 103 ug/kg 03/07/23 00:07 100-41-403/06/23 20:386.9 3.2 1
Hexachloro-1,3-butadiene ND ug/kg 03/07/23 00:07 87-68-303/06/23 20:3813.7 11.2 1
2-Hexanone ND ug/kg 03/07/23 00:07 591-78-603/06/23 20:3868.6 6.6 1
Isopropylbenzene (Cumene)ND ug/kg 03/07/23 00:07 98-82-803/06/23 20:386.9 2.3 1
p-Isopropyltoluene 1720 ug/kg 03/07/23 00:07 99-87-603/06/23 20:386.9 3.4 1
Methylene Chloride ND ug/kg 03/07/23 00:07 75-09-203/06/23 20:3827.4 18.8 1
4-Methyl-2-pentanone (MIBK)101 ug/kg 03/07/23 00:07 108-10-103/06/23 20:3868.6 6.6 1
Methyl-tert-butyl ether ND ug/kg 03/07/23 00:07 1634-04-403/06/23 20:386.9 2.6 1
Naphthalene 654 ug/kg 03/07/23 00:07 91-20-303/06/23 20:386.9 3.6 1
n-Propylbenzene 504 ug/kg 03/07/23 00:07 103-65-103/06/23 20:386.9 2.4 1
Styrene ND ug/kg 03/07/23 00:07 100-42-5 IK03/06/23 20:386.9 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/07/23 00:07 630-20-603/06/23 20:386.9 2.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/07/23 00:07 79-34-503/06/23 20:386.9 1.8 1
Tetrachloroethene 8.5 ug/kg 03/07/23 00:07 127-18-403/06/23 20:386.9 2.2 1
Toluene 179 ug/kg 03/07/23 00:07 108-88-303/06/23 20:386.9 4.7 1
1,2,3-Trichlorobenzene ND ug/kg 03/07/23 00:07 87-61-603/06/23 20:386.9 5.5 1
1,2,4-Trichlorobenzene ND ug/kg 03/07/23 00:07 120-82-103/06/23 20:386.9 5.8 1
1,1,1-Trichloroethane ND ug/kg 03/07/23 00:07 71-55-603/06/23 20:386.9 3.6 1
1,1,2-Trichloroethane ND ug/kg 03/07/23 00:07 79-00-503/06/23 20:386.9 2.3 1
Trichloroethene ND ug/kg 03/07/23 00:07 79-01-603/06/23 20:386.9 5.5 1
Trichlorofluoromethane ND ug/kg 03/07/23 00:07 75-69-403/06/23 20:386.9 3.8 1
1,2,3-Trichloropropane ND ug/kg 03/07/23 00:07 96-18-403/06/23 20:386.9 3.5 1
1,2,4-Trimethylbenzene 5870 ug/kg 03/07/23 00:07 95-63-603/06/23 20:386.9 4.1 1
1,3,5-Trimethylbenzene 2390 ug/kg 03/07/23 00:07 108-67-803/06/23 20:386.9 2.3 1
Vinyl acetate ND ug/kg 03/07/23 00:07 108-05-403/06/23 20:3868.6 14.1 1
Vinyl chloride ND ug/kg 03/07/23 00:07 75-01-403/06/23 20:3813.7 3.5 1
Xylene (Total)795 ug/kg 03/07/23 00:07 1330-20-703/06/23 20:3813.7 3.9 1
m&p-Xylene 475 ug/kg 03/07/23 00:07 179601-23-103/06/23 20:3813.7 4.7 1
o-Xylene 320 ug/kg 03/07/23 00:07 95-47-603/06/23 20:386.9 3.0 1
Surrogates
Toluene-d8 (S)104 %03/07/23 00:07 2037-26-503/06/23 20:3870-130 1
4-Bromofluorobenzene (S)187 %03/07/23 00:07 460-00-4 S503/06/23 20:3870-130 1
1,2-Dichloroethane-d4 (S)117 %03/07/23 00:07 17060-07-003/06/23 20:3870-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.6 %03/06/23 18:04 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655319
NST .001-002
Sample:SB-3A (7-9)Lab ID:92655319002 Collected:03/06/23 13:55 Received:03/06/23 15:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 03/10/23 15:18 N203/09/23 00:0012.0 12.0 1
Aliphatic (C19-C36)ND mg/kg 03/10/23 15:18 N203/09/23 00:0012.0 12.0 1
Aromatic (C11-C22)ND mg/kg 03/10/23 15:18 N203/09/23 00:0012.0 12.0 1
Surrogates
1-Chlorooctadecane (S)68 %03/10/23 15:18 3386-33-203/09/23 00:0040-140 1
o-Terphenyl (S)75 %03/10/23 15:18 84-15-103/09/23 00:0040-140 1
2-Fluorobiphenyl (S)80 %03/10/23 15:18 321-60-803/09/23 00:0040-140 1
2-Bromonaphthalene (S)85 %03/10/23 15:18 580-13-203/09/23 00:0040-140 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.9 %03/07/23 15:04 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655319
NST .001-002
Sample:SB-3A (14-16)Lab ID:92655319003 Collected:03/06/23 14:05 Received:03/06/23 15:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 03/10/23 15:43 N203/09/23 00:0011.9 11.9 1
Aliphatic (C19-C36)ND mg/kg 03/10/23 15:43 N203/09/23 00:0011.9 11.9 1
Aromatic (C11-C22)ND mg/kg 03/10/23 15:43 N203/09/23 00:0011.9 11.9 1
Surrogates
1-Chlorooctadecane (S)68 %03/10/23 15:43 3386-33-203/09/23 00:0040-140 1
o-Terphenyl (S)69 %03/10/23 15:43 84-15-103/09/23 00:0040-140 1
2-Fluorobiphenyl (S)77 %03/10/23 15:43 321-60-803/09/23 00:0040-140 1
2-Bromonaphthalene (S)81 %03/10/23 15:43 580-13-203/09/23 00:0040-140 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.0 %03/07/23 15:04 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655319
NST .001-002
Sample:SB-3A (21-23)Lab ID:92655319004 Collected:03/06/23 14:15 Received:03/06/23 15:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 03/10/23 16:08 N203/09/23 00:0012.6 12.6 1
Aliphatic (C19-C36)ND mg/kg 03/10/23 16:08 N203/09/23 00:0012.6 12.6 1
Aromatic (C11-C22)ND mg/kg 03/10/23 16:08 N203/09/23 00:0012.6 12.6 1
Surrogates
1-Chlorooctadecane (S)60 %03/10/23 16:08 3386-33-203/09/23 00:0040-140 1
o-Terphenyl (S)68 %03/10/23 16:08 84-15-103/09/23 00:0040-140 1
2-Fluorobiphenyl (S)76 %03/10/23 16:08 321-60-803/09/23 00:0040-140 1
2-Bromonaphthalene (S)80 %03/10/23 16:08 580-13-203/09/23 00:0040-140 1
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Chromium 21.7 mg/kg 03/09/23 17:43 7440-47-303/09/23 10:342.5 0.49 1
Lead 13.8 mg/kg 03/09/23 17:43 7439-92-103/09/23 10:340.63 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 03/08/23 17:54 83-32-903/07/23 09:434181471
Acenaphthylene ND ug/kg 03/08/23 17:54 208-96-803/07/23 09:434181471
Aniline ND ug/kg 03/08/23 17:54 62-53-303/07/23 09:434181641
Anthracene ND ug/kg 03/08/23 17:54 120-12-703/07/23 09:434181371
Benzo(a)anthracene ND ug/kg 03/08/23 17:54 56-55-303/07/23 09:434181391
Benzo(a)pyrene ND ug/kg 03/08/23 17:54 50-32-803/07/23 09:434181441
Benzo(b)fluoranthene ND ug/kg 03/08/23 17:54 205-99-203/07/23 09:434181391
Benzo(g,h,i)perylene ND ug/kg 03/08/23 17:54 191-24-203/07/23 09:434181621
Benzo(k)fluoranthene ND ug/kg 03/08/23 17:54 207-08-903/07/23 09:434181471
Benzoic Acid ND ug/kg 03/08/23 17:54 65-85-003/07/23 09:4320908991
Benzyl alcohol ND ug/kg 03/08/23 17:54 100-51-603/07/23 09:438373171
4-Bromophenylphenyl ether ND ug/kg 03/08/23 17:54 101-55-303/07/23 09:434181611
Butylbenzylphthalate ND ug/kg 03/08/23 17:54 85-68-703/07/23 09:434181761
4-Chloro-3-methylphenol ND ug/kg 03/08/23 17:54 59-50-703/07/23 09:438372941
4-Chloroaniline ND ug/kg 03/08/23 17:54 106-47-803/07/23 09:438373281
bis(2-Chloroethoxy)methane ND ug/kg 03/08/23 17:54 111-91-103/07/23 09:434181741
bis(2-Chloroethyl) ether ND ug/kg 03/08/23 17:54 111-44-403/07/23 09:434181571
2-Chloronaphthalene ND ug/kg 03/08/23 17:54 91-58-703/07/23 09:434181661
2-Chlorophenol ND ug/kg 03/08/23 17:54 95-57-803/07/23 09:434181571
4-Chlorophenylphenyl ether ND ug/kg 03/08/23 17:54 7005-72-303/07/23 09:434181561
Chrysene ND ug/kg 03/08/23 17:54 218-01-903/07/23 09:434181521
Dibenz(a,h)anthracene ND ug/kg 03/08/23 17:54 53-70-303/07/23 09:434181611
Dibenzofuran ND ug/kg 03/08/23 17:54 132-64-903/07/23 09:434181511
1,2-Dichlorobenzene ND ug/kg 03/08/23 17:54 95-50-103/07/23 09:434181511
1,3-Dichlorobenzene ND ug/kg 03/08/23 17:54 541-73-103/07/23 09:434181481
1,4-Dichlorobenzene ND ug/kg 03/08/23 17:54 106-46-703/07/23 09:434181601
3,3'-Dichlorobenzidine ND ug/kg 03/08/23 17:54 91-94-103/07/23 09:438372831
2,4-Dichlorophenol ND ug/kg 03/08/23 17:54 120-83-203/07/23 09:434181641
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655319
NST .001-002
Sample:SB-3A (21-23)Lab ID:92655319004 Collected:03/06/23 14:15 Received:03/06/23 15:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Diethylphthalate ND ug/kg 03/08/23 17:54 84-66-203/07/23 09:434181531
2,4-Dimethylphenol ND ug/kg 03/08/23 17:54 105-67-903/07/23 09:434181741
Dimethylphthalate ND ug/kg 03/08/23 17:54 131-11-303/07/23 09:434181521
Di-n-butylphthalate ND ug/kg 03/08/23 17:54 84-74-203/07/23 09:434181411
4,6-Dinitro-2-methylphenol ND ug/kg 03/08/23 17:54 534-52-103/07/23 09:438373901
2,4-Dinitrophenol ND ug/kg 03/08/23 17:54 51-28-503/07/23 09:43209012901
2,4-Dinitrotoluene ND ug/kg 03/08/23 17:54 121-14-203/07/23 09:434181611
2,6-Dinitrotoluene ND ug/kg 03/08/23 17:54 606-20-203/07/23 09:434181531
Di-n-octylphthalate ND ug/kg 03/08/23 17:54 117-84-003/07/23 09:434181651
bis(2-Ethylhexyl)phthalate ND ug/kg 03/08/23 17:54 117-81-703/07/23 09:434181621
Fluoranthene ND ug/kg 03/08/23 17:54 206-44-003/07/23 09:434181431
Fluorene ND ug/kg 03/08/23 17:54 86-73-703/07/23 09:434181471
Hexachloro-1,3-butadiene ND ug/kg 03/08/23 17:54 87-68-303/07/23 09:434181811
Hexachlorobenzene ND ug/kg 03/08/23 17:54 118-74-103/07/23 09:434181641
Hexachlorocyclopentadiene ND ug/kg 03/08/23 17:54 77-47-403/07/23 09:434182401
Hexachloroethane ND ug/kg 03/08/23 17:54 67-72-103/07/23 09:434181601
Indeno(1,2,3-cd)pyrene ND ug/kg 03/08/23 17:54 193-39-503/07/23 09:434181651
Isophorone ND ug/kg 03/08/23 17:54 78-59-103/07/23 09:434181861
1-Methylnaphthalene ND ug/kg 03/08/23 17:54 90-12-003/07/23 09:434181471
2-Methylnaphthalene ND ug/kg 03/08/23 17:54 91-57-603/07/23 09:434181671
2-Methylphenol(o-Cresol)ND ug/kg 03/08/23 17:54 95-48-703/07/23 09:434181711
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/08/23 17:54 15831-10-403/07/23 09:434181691
Naphthalene ND ug/kg 03/08/23 17:54 91-20-303/07/23 09:434181421
2-Nitroaniline ND ug/kg 03/08/23 17:54 88-74-403/07/23 09:4320903421
3-Nitroaniline ND ug/kg 03/08/23 17:54 99-09-203/07/23 09:4320903281
4-Nitroaniline ND ug/kg 03/08/23 17:54 100-01-603/07/23 09:438373181
Nitrobenzene ND ug/kg 03/08/23 17:54 98-95-303/07/23 09:434181941
2-Nitrophenol ND ug/kg 03/08/23 17:54 88-75-503/07/23 09:434181811
4-Nitrophenol ND ug/kg 03/08/23 17:54 100-02-703/07/23 09:4320908091
N-Nitrosodimethylamine ND ug/kg 03/08/23 17:54 62-75-903/07/23 09:434181411
N-Nitroso-di-n-propylamine ND ug/kg 03/08/23 17:54 621-64-703/07/23 09:434181571
N-Nitrosodiphenylamine ND ug/kg 03/08/23 17:54 86-30-603/07/23 09:434181481
2,2'-Oxybis(1-chloropropane)ND ug/kg 03/08/23 17:54 108-60-103/07/23 09:434181991
Pentachlorophenol ND ug/kg 03/08/23 17:54 87-86-503/07/23 09:438374091
Phenanthrene ND ug/kg 03/08/23 17:54 85-01-803/07/23 09:434181371
Phenol ND ug/kg 03/08/23 17:54 108-95-203/07/23 09:434181861
Pyrene ND ug/kg 03/08/23 17:54 129-00-003/07/23 09:434181701
Pyridine ND ug/kg 03/08/23 17:54 110-86-103/07/23 09:434181321
1,2,4-Trichlorobenzene ND ug/kg 03/08/23 17:54 120-82-103/07/23 09:434181651
2,4,5-Trichlorophenol ND ug/kg 03/08/23 17:54 95-95-403/07/23 09:434181911
2,4,6-Trichlorophenol ND ug/kg 03/08/23 17:54 88-06-203/07/23 09:434181721
Surrogates
Nitrobenzene-d5 (S)59 %03/08/23 17:54 4165-60-003/07/23 09:4310-130 1
2-Fluorobiphenyl (S)53 %03/08/23 17:54 321-60-803/07/23 09:4310-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655319
NST .001-002
Sample:SB-3A (21-23)Lab ID:92655319004 Collected:03/06/23 14:15 Received:03/06/23 15:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Terphenyl-d14 (S)57 %03/08/23 17:54 1718-51-003/07/23 09:4310-130 1
Phenol-d6 (S)52 %03/08/23 17:54 13127-88-303/07/23 09:4310-130 1
2-Fluorophenol (S)49 %03/08/23 17:54 367-12-403/07/23 09:4310-130 1
2,4,6-Tribromophenol (S)59 %03/08/23 17:54 118-79-603/07/23 09:4310-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 03/09/23 10:28 67-64-1 v203/08/23 15:3116051.3 1
Benzene ND ug/kg 03/09/23 10:28 71-43-203/08/23 15:318.0 3.2 1
Bromobenzene ND ug/kg 03/09/23 10:28 108-86-103/08/23 15:318.0 2.6 1
Bromochloromethane ND ug/kg 03/09/23 10:28 74-97-503/08/23 15:318.0 2.4 1
Bromodichloromethane ND ug/kg 03/09/23 10:28 75-27-403/08/23 15:318.0 3.1 1
Bromoform ND ug/kg 03/09/23 10:28 75-25-203/08/23 15:318.0 2.8 1
Bromomethane ND ug/kg 03/09/23 10:28 74-83-9 v203/08/23 15:3131.9 24.8 1
2-Butanone (MEK)ND ug/kg 03/09/23 10:28 78-93-303/08/23 15:3116038.3 1
n-Butylbenzene ND ug/kg 03/09/23 10:28 104-51-803/08/23 15:318.0 5.0 1
sec-Butylbenzene ND ug/kg 03/09/23 10:28 135-98-803/08/23 15:318.0 3.5 1
tert-Butylbenzene ND ug/kg 03/09/23 10:28 98-06-603/08/23 15:318.0 2.8 1
Carbon tetrachloride ND ug/kg 03/09/23 10:28 56-23-5 IK03/08/23 15:318.0 3.0 1
Chlorobenzene ND ug/kg 03/09/23 10:28 108-90-703/08/23 15:318.0 4.6 1
Chloroethane ND ug/kg 03/09/23 10:28 75-00-3 v203/08/23 15:3116.0 6.2 1
Chloroform ND ug/kg 03/09/23 10:28 67-66-303/08/23 15:318.0 6.7 1
Chloromethane ND ug/kg 03/09/23 10:28 74-87-303/08/23 15:3116.0 6.7 1
2-Chlorotoluene ND ug/kg 03/09/23 10:28 95-49-803/08/23 15:318.0 2.8 1
4-Chlorotoluene ND ug/kg 03/09/23 10:28 106-43-403/08/23 15:318.0 4.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/09/23 10:28 96-12-803/08/23 15:318.0 3.1 1
Dibromochloromethane ND ug/kg 03/09/23 10:28 124-48-1 IK03/08/23 15:318.0 4.5 1
1,2-Dibromoethane (EDB)ND ug/kg 03/09/23 10:28 106-93-403/08/23 15:318.0 3.5 1
Dibromomethane ND ug/kg 03/09/23 10:28 74-95-303/08/23 15:318.0 1.7 1
1,2-Dichlorobenzene ND ug/kg 03/09/23 10:28 95-50-103/08/23 15:318.0 2.9 1
1,3-Dichlorobenzene ND ug/kg 03/09/23 10:28 541-73-103/08/23 15:318.0 2.5 1
1,4-Dichlorobenzene ND ug/kg 03/09/23 10:28 106-46-703/08/23 15:318.0 2.1 1
Dichlorodifluoromethane ND ug/kg 03/09/23 10:28 75-71-803/08/23 15:3116.0 8.1 1
1,1-Dichloroethane ND ug/kg 03/09/23 10:28 75-34-303/08/23 15:318.0 3.3 1
1,2-Dichloroethane ND ug/kg 03/09/23 10:28 107-06-203/08/23 15:318.0 5.3 1
1,1-Dichloroethene ND ug/kg 03/09/23 10:28 75-35-403/08/23 15:318.0 3.3 1
cis-1,2-Dichloroethene ND ug/kg 03/09/23 10:28 156-59-203/08/23 15:318.0 2.7 1
trans-1,2-Dichloroethene ND ug/kg 03/09/23 10:28 156-60-503/08/23 15:318.0 6.8 1
1,2-Dichloropropane ND ug/kg 03/09/23 10:28 78-87-503/08/23 15:318.0 2.4 1
1,3-Dichloropropane ND ug/kg 03/09/23 10:28 142-28-903/08/23 15:318.0 2.5 1
2,2-Dichloropropane ND ug/kg 03/09/23 10:28 594-20-7 v203/08/23 15:318.0 6.1 1
1,1-Dichloropropene ND ug/kg 03/09/23 10:28 563-58-603/08/23 15:318.0 3.8 1
cis-1,3-Dichloropropene ND ug/kg 03/09/23 10:28 10061-01-503/08/23 15:318.0 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655319
NST .001-002
Sample:SB-3A (21-23)Lab ID:92655319004 Collected:03/06/23 14:15 Received:03/06/23 15:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
trans-1,3-Dichloropropene ND ug/kg 03/09/23 10:28 10061-02-603/08/23 15:318.0 2.7 1
Diisopropyl ether ND ug/kg 03/09/23 10:28 108-20-303/08/23 15:318.0 2.2 1
Ethylbenzene ND ug/kg 03/09/23 10:28 100-41-403/08/23 15:318.0 3.7 1
Hexachloro-1,3-butadiene ND ug/kg 03/09/23 10:28 87-68-303/08/23 15:3116.0 13.1 1
2-Hexanone ND ug/kg 03/09/23 10:28 591-78-6 v203/08/23 15:3179.9 7.7 1
Isopropylbenzene (Cumene)ND ug/kg 03/09/23 10:28 98-82-803/08/23 15:318.0 2.7 1
p-Isopropyltoluene ND ug/kg 03/09/23 10:28 99-87-603/08/23 15:318.0 3.9 1
Methylene Chloride ND ug/kg 03/09/23 10:28 75-09-203/08/23 15:3131.9 21.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/09/23 10:28 108-10-1 v203/08/23 15:3179.9 7.7 1
Methyl-tert-butyl ether ND ug/kg 03/09/23 10:28 1634-04-403/08/23 15:318.0 3.0 1
Naphthalene ND ug/kg 03/09/23 10:28 91-20-3 M103/08/23 15:318.0 4.2 1
n-Propylbenzene ND ug/kg 03/09/23 10:28 103-65-103/08/23 15:318.0 2.8 1
Styrene ND ug/kg 03/09/23 10:28 100-42-5 IK03/08/23 15:318.0 2.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/09/23 10:28 630-20-603/08/23 15:318.0 3.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/09/23 10:28 79-34-503/08/23 15:318.0 2.1 1
Tetrachloroethene ND ug/kg 03/09/23 10:28 127-18-403/08/23 15:318.0 2.5 1
Toluene ND ug/kg 03/09/23 10:28 108-88-303/08/23 15:318.0 5.5 1
1,2,3-Trichlorobenzene ND ug/kg 03/09/23 10:28 87-61-6 M103/08/23 15:318.0 6.5 1
1,2,4-Trichlorobenzene ND ug/kg 03/09/23 10:28 120-82-103/08/23 15:318.0 6.7 1
1,1,1-Trichloroethane ND ug/kg 03/09/23 10:28 71-55-603/08/23 15:318.0 4.2 1
1,1,2-Trichloroethane ND ug/kg 03/09/23 10:28 79-00-503/08/23 15:318.0 2.7 1
Trichloroethene ND ug/kg 03/09/23 10:28 79-01-603/08/23 15:318.0 6.4 1
Trichlorofluoromethane ND ug/kg 03/09/23 10:28 75-69-403/08/23 15:318.0 4.4 1
1,2,3-Trichloropropane ND ug/kg 03/09/23 10:28 96-18-403/08/23 15:318.0 4.0 1
1,2,4-Trimethylbenzene ND ug/kg 03/09/23 10:28 95-63-603/08/23 15:318.0 4.7 1
1,3,5-Trimethylbenzene ND ug/kg 03/09/23 10:28 108-67-803/08/23 15:318.0 2.7 1
Vinyl acetate ND ug/kg 03/09/23 10:28 108-05-403/08/23 15:3179.9 16.4 1
Vinyl chloride ND ug/kg 03/09/23 10:28 75-01-403/08/23 15:3116.0 4.1 1
Xylene (Total)ND ug/kg 03/09/23 10:28 1330-20-703/08/23 15:3116.0 4.6 1
m&p-Xylene ND ug/kg 03/09/23 10:28 179601-23-103/08/23 15:3116.0 5.5 1
o-Xylene ND ug/kg 03/09/23 10:28 95-47-603/08/23 15:318.0 3.5 1
Surrogates
Toluene-d8 (S)101 %03/09/23 10:28 2037-26-503/08/23 15:3170-130 1
4-Bromofluorobenzene (S)108 %03/09/23 10:28 460-00-403/08/23 15:3170-130 1
1,2-Dichloroethane-d4 (S)99 %03/09/23 10:28 17060-07-003/08/23 15:3170-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.8 %03/07/23 15:04 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655319
NST .001-002
Sample:TMW-2A Lab ID:92655319005 Collected:03/06/23 12:55 Received:03/06/23 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 03/08/23 19:42 N203/07/23 16:3297.1 97.1 1
Aliphatic (C19-C36)ND ug/L 03/08/23 19:42 N203/07/23 16:3297.1 97.1 1
Aromatic (C11-C22)ND ug/L 03/08/23 19:42 N203/07/23 16:3297.1 97.1 1
Surrogates
1-Chlorooctadecane (S)67 %03/08/23 19:42 3386-33-203/07/23 16:3240-140 1
o-Terphenyl (S)82 %03/08/23 19:42 84-15-103/07/23 16:3240-140 1
2-Fluorobiphenyl (S)106 %03/08/23 19:42 321-60-803/07/23 16:3240-140 1
2-Bromonaphthalene (S)109 %03/08/23 19:42 580-13-203/07/23 16:3240-140 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Chromium 0.60J ug/L 03/14/23 17:43 7440-47-303/10/23 12:231.0 0.50 1
Lead 0.32J ug/L 03/14/23 17:43 7439-92-103/10/23 12:231.0 0.077 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 03/09/23 17:18 83-32-903/09/23 10:195.0 2.0 1
Acenaphthylene ND ug/L 03/09/23 17:18 208-96-803/09/23 10:195.0 2.0 1
Anthracene ND ug/L 03/09/23 17:18 120-12-703/09/23 10:195.0 2.3 1
Benzo(a)anthracene ND ug/L 03/09/23 17:18 56-55-303/09/23 10:195.0 2.7 1
Benzo(a)pyrene ND ug/L 03/09/23 17:18 50-32-803/09/23 10:195.0 2.8 1
Benzo(b)fluoranthene ND ug/L 03/09/23 17:18 205-99-203/09/23 10:195.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 03/09/23 17:18 191-24-203/09/23 10:195.0 2.8 1
Benzo(k)fluoranthene ND ug/L 03/09/23 17:18 207-08-903/09/23 10:195.0 2.7 1
4-Bromophenylphenyl ether ND ug/L 03/09/23 17:18 101-55-303/09/23 10:195.0 1.8 1
Butylbenzylphthalate ND ug/L 03/09/23 17:18 85-68-703/09/23 10:195.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 03/09/23 17:18 59-50-703/09/23 10:195.0 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 03/09/23 17:18 111-91-103/09/23 10:1910.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 03/09/23 17:18 111-44-403/09/23 10:195.0 1.9 1
2-Chloronaphthalene ND ug/L 03/09/23 17:18 91-58-703/09/23 10:195.0 1.7 1
2-Chlorophenol ND ug/L 03/09/23 17:18 95-57-803/09/23 10:195.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 03/09/23 17:18 7005-72-303/09/23 10:195.0 2.0 1
Chrysene ND ug/L 03/09/23 17:18 218-01-903/09/23 10:195.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 03/09/23 17:18 53-70-303/09/23 10:195.0 3.0 1
3,3'-Dichlorobenzidine ND ug/L 03/09/23 17:18 91-94-103/09/23 10:1910.0 8.1 1
2,4-Dichlorophenol ND ug/L 03/09/23 17:18 120-83-203/09/23 10:195.0 1.4 1
Diethylphthalate ND ug/L 03/09/23 17:18 84-66-203/09/23 10:195.0 2.0 1
2,4-Dimethylphenol ND ug/L 03/09/23 17:18 105-67-903/09/23 10:1910.0 1.7 1
Dimethylphthalate ND ug/L 03/09/23 17:18 131-11-303/09/23 10:195.0 2.1 1
Di-n-butylphthalate ND ug/L 03/09/23 17:18 84-74-203/09/23 10:195.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 03/09/23 17:18 534-52-103/09/23 10:1910.0 7.8 1
2,4-Dinitrophenol ND ug/L 03/09/23 17:18 51-28-503/09/23 10:1950.0 26.0 1
2,4-Dinitrotoluene ND ug/L 03/09/23 17:18 121-14-203/09/23 10:195.0 1.6 1
2,6-Dinitrotoluene ND ug/L 03/09/23 17:18 606-20-203/09/23 10:195.0 1.7 1
Di-n-octylphthalate ND ug/L 03/09/23 17:18 117-84-003/09/23 10:195.0 3.9 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
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Page 15 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655319
NST .001-002
Sample:TMW-2A Lab ID:92655319005 Collected:03/06/23 12:55 Received:03/06/23 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
bis(2-Ethylhexyl)phthalate ND ug/L 03/09/23 17:18 117-81-703/09/23 10:195.0 3.7 1
Fluoranthene ND ug/L 03/09/23 17:18 206-44-003/09/23 10:195.0 2.2 1
Fluorene ND ug/L 03/09/23 17:18 86-73-703/09/23 10:195.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 03/09/23 17:18 87-68-303/09/23 10:195.0 1.8 1
Hexachlorobenzene ND ug/L 03/09/23 17:18 118-74-103/09/23 10:195.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 03/09/23 17:18 77-47-403/09/23 10:1910.0 1.6 1
Hexachloroethane ND ug/L 03/09/23 17:18 67-72-103/09/23 10:195.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/09/23 17:18 193-39-503/09/23 10:195.0 2.9 1
Isophorone ND ug/L 03/09/23 17:18 78-59-103/09/23 10:1910.0 1.7 1
Naphthalene 3.2J ug/L 03/09/23 17:18 91-20-303/09/23 10:195.0 2.1 1
Nitrobenzene ND ug/L 03/09/23 17:18 98-95-303/09/23 10:195.0 1.9 1
2-Nitrophenol ND ug/L 03/09/23 17:18 88-75-503/09/23 10:195.0 1.4 1
4-Nitrophenol ND ug/L 03/09/23 17:18 100-02-703/09/23 10:1910.0 6.6 1
N-Nitrosodimethylamine ND ug/L 03/09/23 17:18 62-75-903/09/23 10:195.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 03/09/23 17:18 621-64-703/09/23 10:195.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/09/23 17:18 86-30-603/09/23 10:1910.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/09/23 17:18 108-60-103/09/23 10:195.0 1.2 1
Pentachlorophenol ND ug/L 03/09/23 17:18 87-86-503/09/23 10:1910.0 3.8 1
Phenanthrene ND ug/L 03/09/23 17:18 85-01-803/09/23 10:195.0 2.0 1
Phenol ND ug/L 03/09/23 17:18 108-95-203/09/23 10:195.0 1.4 1
Pyrene ND ug/L 03/09/23 17:18 129-00-003/09/23 10:195.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 03/09/23 17:18 120-82-103/09/23 10:195.0 1.7 1
2,4,6-Trichlorophenol ND ug/L 03/09/23 17:18 88-06-203/09/23 10:1910.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)62 %03/09/23 17:18 4165-60-003/09/23 10:1910-120 1
2-Fluorobiphenyl (S)57 %03/09/23 17:18 321-60-803/09/23 10:1915-120 1
Terphenyl-d14 (S)119 %03/09/23 17:18 1718-51-003/09/23 10:1911-131 1
Phenol-d6 (S)38 %03/09/23 17:18 13127-88-303/09/23 10:1910-120 1
2-Fluorophenol (S)48 %03/09/23 17:18 367-12-403/09/23 10:1910-120 1
2,4,6-Tribromophenol (S)95 %03/09/23 17:18 118-79-603/09/23 10:1910-137 1
Tentatively Identified Compounds
Unknown 10.6J ug/L 03/09/23 17:1803/09/23 10:191
Toluene 78.8J ug/L 03/09/23 17:18 108-88-3 N03/09/23 10:191
Ethylbenzene 13.7J ug/L 03/09/23 17:18 100-41-4 N03/09/23 10:191
p-Xylene 44.1J ug/L 03/09/23 17:18 106-42-3 N03/09/23 10:191
p-Xylene 20.7J ug/L 03/09/23 17:18 106-42-3 N03/09/23 10:191
Benzene, 1-ethyl-3-methy 11.6J ug/L 03/09/23 17:18 620-14-4 N03/09/23 10:191
n-Hexadecanoic acid 5.8J ug/L 03/09/23 17:18 57-10-3 N03/09/23 10:191
Unknown 8.4J ug/L 03/09/23 17:1803/09/23 10:191
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 03/08/23 12:38 71-43-20.50 0.34 1
Bromobenzene ND ug/L 03/08/23 12:38 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 03/08/23 12:38 74-97-50.50 0.47 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
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[phone]
Page 16 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655319
NST .001-002
Sample:TMW-2A Lab ID:92655319005 Collected:03/06/23 12:55 Received:03/06/23 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Bromodichloromethane ND ug/L 03/08/23 12:38 75-27-40.50 0.31 1
Bromoform ND ug/L 03/08/23 12:38 75-25-20.50 0.34 1
Bromomethane ND ug/L 03/08/23 12:38 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 03/08/23 12:38 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 03/08/23 12:38 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 03/08/23 12:38 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 03/08/23 12:38 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 03/08/23 12:38 108-90-70.50 0.28 1
Chloroethane ND ug/L 03/08/23 12:38 75-00-31.0 0.65 1
Chloroform ND ug/L 03/08/23 12:38 67-66-30.50 0.43 1
Chloromethane ND ug/L 03/08/23 12:38 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 03/08/23 12:38 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 03/08/23 12:38 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 03/08/23 12:38 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 03/08/23 12:38 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 03/08/23 12:38 106-93-40.50 0.27 1
Dibromomethane ND ug/L 03/08/23 12:38 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 03/08/23 12:38 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 03/08/23 12:38 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 03/08/23 12:38 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 03/08/23 12:38 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 03/08/23 12:38 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 03/08/23 12:38 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 03/08/23 12:38 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 03/08/23 12:38 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 03/08/23 12:38 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 03/08/23 12:38 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 03/08/23 12:38 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 03/08/23 12:38 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 03/08/23 12:38 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 03/08/23 12:38 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 03/08/23 12:38 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 03/08/23 12:38 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 03/08/23 12:38 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/08/23 12:38 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 03/08/23 12:38 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 03/08/23 12:38 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 03/08/23 12:38 1634-04-40.50 0.42 1
Naphthalene 1.5J ug/L 03/08/23 12:38 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 03/08/23 12:38 103-65-10.50 0.34 1
Styrene ND ug/L 03/08/23 12:38 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 03/08/23 12:38 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 03/08/23 12:38 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 03/08/23 12:38 127-18-40.50 0.29 1
Toluene ND ug/L 03/08/23 12:38 108-88-30.50 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92655319
NST .001-002
Sample:TMW-2A Lab ID:92655319005 Collected:03/06/23 12:55 Received:03/06/23 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2,3-Trichlorobenzene ND ug/L 03/08/23 12:38 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 03/08/23 12:38 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 03/08/23 12:38 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 03/08/23 12:38 79-00-50.50 0.32 1
Trichloroethene ND ug/L 03/08/23 12:38 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 03/08/23 12:38 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 03/08/23 12:38 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene 1.7 ug/L 03/08/23 12:38 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene 0.72 ug/L 03/08/23 12:38 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 03/08/23 12:38 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 03/08/23 12:38 179601-23-11.0 0.71 1
o-Xylene ND ug/L 03/08/23 12:38 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %03/08/23 12:38 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %03/08/23 12:38 460-00-470-130 1
Toluene-d8 (S)105 %03/08/23 12:38 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
760673
EPA 3010A
EPA 6020B
6020 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92655319005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3951289
Associated Lab Samples:92655319005
Matrix:Water
AnalyzedMDL
Chromium ug/L ND 1.0 03/14/23 17:360.50
Lead ug/L ND 1.0 03/14/23 17:360.077
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3951290LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium ug/L 52.650 105 80-120
Lead ug/L 51.250 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3951291MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92655319005
3951292
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium ug/L 50 104 75-125104 0 20500.60J 52.5 52.7
Lead ug/L 50 102 75-125101 0 20500.32J 51.1 51.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
870506
EPA 3050B
EPA 6020B
6020B Solids UPD5
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples:92655319001, 92655319004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4591450
Associated Lab Samples:92655319001, 92655319004
Matrix:Solid
AnalyzedMDL
Chromium mg/kg ND 2.0 03/09/23 17:080.39
Lead mg/kg ND 0.50 03/09/23 17:080.092
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4591451LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium mg/kg 55.449.6 112 80-120
Lead mg/kg 51.249.6 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4591452MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92655319001
4591453
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium mg/kg M1,R161.2 138 75-12546 43 2061.175.5 160 104
Lead mg/kg 61.2 105 75-125103 2 2061.112.7 76.9 75.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
760113
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92655319005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3947783
Associated Lab Samples:92655319005
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 03/08/23 11:450.31
1,1,1-Trichloroethane ug/L ND 0.50 03/08/23 11:450.33
1,1,2,2-Tetrachloroethane ug/L ND 0.50 03/08/23 11:450.22
1,1,2-Trichloroethane ug/L ND 0.50 03/08/23 11:450.32
1,1-Dichloroethane ug/L ND 0.50 03/08/23 11:450.37
1,1-Dichloroethene ug/L ND 0.50 03/08/23 11:450.35
1,1-Dichloropropene ug/L ND 0.50 03/08/23 11:450.43
1,2,3-Trichlorobenzene ug/L ND 2.0 03/08/23 11:450.81
1,2,3-Trichloropropane ug/L ND 0.50 03/08/23 11:450.26
1,2,4-Trichlorobenzene ug/L ND 2.0 03/08/23 11:450.64
1,2,4-Trimethylbenzene ug/L ND 0.50 03/08/23 11:450.50
1,2-Dibromo-3-chloropropane ug/L ND 1.0 03/08/23 11:450.34
1,2-Dibromoethane (EDB)ug/L ND 0.50 03/08/23 11:450.27
1,2-Dichlorobenzene ug/L ND 0.50 03/08/23 11:450.34
1,2-Dichloroethane ug/L ND 0.50 03/08/23 11:450.32
1,2-Dichloropropane ug/L ND 0.50 03/08/23 11:450.36
1,3,5-Trimethylbenzene ug/L ND 0.50 03/08/23 11:450.33
1,3-Dichlorobenzene ug/L ND 0.50 03/08/23 11:450.34
1,3-Dichloropropane ug/L ND 0.50 03/08/23 11:450.28
1,4-Dichlorobenzene ug/L ND 0.50 03/08/23 11:450.33
2,2-Dichloropropane ug/L ND 0.50 03/08/23 11:450.39
2-Chlorotoluene ug/L ND 0.50 03/08/23 11:450.32
4-Chlorotoluene ug/L ND 0.50 03/08/23 11:450.32
Benzene ug/L ND 0.50 03/08/23 11:450.34
Bromobenzene ug/L ND 0.50 03/08/23 11:450.29
Bromochloromethane ug/L ND 0.50 03/08/23 11:450.47
Bromodichloromethane ug/L ND 0.50 03/08/23 11:450.31
Bromoform ug/L ND 0.50 03/08/23 11:450.34
Bromomethane ug/L ND 5.0 03/08/23 11:451.7
Carbon tetrachloride ug/L ND 0.50 03/08/23 11:450.33
Chlorobenzene ug/L ND 0.50 03/08/23 11:450.28
Chloroethane ug/L ND 1.0 03/08/23 11:450.65
Chloroform ug/L ND 0.50 03/08/23 11:450.43
Chloromethane ug/L ND 1.0 03/08/23 11:450.54
cis-1,2-Dichloroethene ug/L ND 0.50 03/08/23 11:450.38
cis-1,3-Dichloropropene ug/L ND 0.50 03/08/23 11:450.36
Dibromochloromethane ug/L ND 0.50 03/08/23 11:450.36
Dibromomethane ug/L ND 0.50 03/08/23 11:450.39
Dichlorodifluoromethane ug/L ND 0.50 03/08/23 11:450.35
Diisopropyl ether ug/L ND 0.50 03/08/23 11:450.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3947783
Associated Lab Samples:92655319005
Matrix:Water
AnalyzedMDL
Ethylbenzene ug/L ND 0.50 03/08/23 11:450.30
Hexachloro-1,3-butadiene ug/L ND 2.0 03/08/23 11:451.5
Isopropylbenzene (Cumene)ug/L ND 0.50 03/08/23 11:450.33
m&p-Xylene ug/L ND 1.0 03/08/23 11:450.71
Methyl-tert-butyl ether ug/L ND 0.50 03/08/23 11:450.42
Methylene Chloride ug/L ND 2.0 03/08/23 11:452.0
n-Butylbenzene ug/L ND 0.50 03/08/23 11:450.49
n-Propylbenzene ug/L ND 0.50 03/08/23 11:450.34
Naphthalene ug/L ND 2.0 03/08/23 11:450.64
o-Xylene ug/L ND 0.50 03/08/23 11:450.34
sec-Butylbenzene ug/L ND 0.50 03/08/23 11:450.40
Styrene ug/L ND 0.50 03/08/23 11:450.29
tert-Butylbenzene ug/L ND 0.50 03/08/23 11:450.32
Tetrachloroethene ug/L ND 0.50 03/08/23 11:450.29
Toluene ug/L ND 0.50 03/08/23 11:450.24
trans-1,2-Dichloroethene ug/L ND 0.50 03/08/23 11:450.40
trans-1,3-Dichloropropene ug/L ND 0.50 03/08/23 11:450.36
Trichloroethene ug/L ND 0.50 03/08/23 11:450.38
Trichlorofluoromethane ug/L ND 1.0 03/08/23 11:450.30
Vinyl chloride ug/L ND 1.0 03/08/23 11:450.39
1,2-Dichloroethane-d4 (S)%100 70-130 03/08/23 11:45
4-Bromofluorobenzene (S)%102 70-130 03/08/23 11:45
Toluene-d8 (S)%106 70-130 03/08/23 11:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3947784LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 21.720 109 60-140
1,1,1-Trichloroethane ug/L 21.520 107 60-140
1,1,2,2-Tetrachloroethane ug/L 21.220 106 60-140
1,1,2-Trichloroethane ug/L 20.620 103 60-140
1,1-Dichloroethane ug/L 19.720 99 60-140
1,1-Dichloroethene ug/L 21.620 108 60-140
1,1-Dichloropropene ug/L 22.120 111 60-140
1,2,3-Trichlorobenzene ug/L 20.220 101 60-140
1,2,3-Trichloropropane ug/L 20.020 100 60-140
1,2,4-Trichlorobenzene ug/L 20.220 101 60-140
1,2,4-Trimethylbenzene ug/L 20.920 104 60-140
1,2-Dibromo-3-chloropropane ug/L 20.820 104 60-140
1,2-Dibromoethane (EDB)ug/L 21.320 107 60-140
1,2-Dichlorobenzene ug/L 20.620 103 60-140
1,2-Dichloroethane ug/L 22.720 113 60-140
1,2-Dichloropropane ug/L 21.220 106 60-140
1,3,5-Trimethylbenzene ug/L 20.620 103 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3947784LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 20.520 103 60-140
1,3-Dichloropropane ug/L 20.220 101 60-140
1,4-Dichlorobenzene ug/L 19.620 98 60-140
2,2-Dichloropropane ug/L 20.920 104 60-140
2-Chlorotoluene ug/L 20.720 104 60-140
4-Chlorotoluene ug/L 20.820 104 60-140
Benzene ug/L 21.020 105 60-140
Bromobenzene ug/L 20.020 100 60-140
Bromochloromethane ug/L 19.620 98 60-140
Bromodichloromethane ug/L 20.520 103 60-140
Bromoform ug/L 20.920 105 60-140
Bromomethane ug/L 18.520 92 60-140
Carbon tetrachloride ug/L 22.220 111 60-140
Chlorobenzene ug/L 19.920 100 60-140
Chloroethane ug/L 19.120 96 60-140
Chloroform ug/L 20.520 103 60-140
Chloromethane ug/L 22.120 111 60-140
cis-1,2-Dichloroethene ug/L 20.820 104 60-140
cis-1,3-Dichloropropene ug/L 20.420 102 60-140
Dibromochloromethane ug/L 21.420 107 60-140
Dibromomethane ug/L 21.320 106 60-140
Dichlorodifluoromethane ug/L 21.720 109 60-140
Diisopropyl ether ug/L 20.820 104 60-140
Ethylbenzene ug/L 20.220 101 60-140
Hexachloro-1,3-butadiene ug/L 21.020 105 60-140
Isopropylbenzene (Cumene)ug/L 20.920 105 60-140
m&p-Xylene ug/L 40.940 102 60-140
Methyl-tert-butyl ether ug/L 18.820 94 60-140
Methylene Chloride ug/L 20.720 103 60-140
n-Butylbenzene ug/L 20.520 103 60-140
n-Propylbenzene ug/L 20.220 101 60-140
Naphthalene ug/L 20.620 103 60-140
o-Xylene ug/L 20.020 100 60-140
sec-Butylbenzene ug/L 20.320 101 60-140
Styrene ug/L 20.620 103 60-140
tert-Butylbenzene ug/L 16.820 84 60-140
Tetrachloroethene ug/L 20.220 101 60-140
Toluene ug/L 19.320 97 60-140
trans-1,2-Dichloroethene ug/L 20.420 102 60-140
trans-1,3-Dichloropropene ug/L 21.420 107 60-140
Trichloroethene ug/L 20.520 103 60-140
Trichlorofluoromethane ug/L 20.920 105 60-140
Vinyl chloride ug/L 17.220 86 60-140
1,2-Dichloroethane-d4 (S)%112 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3947785MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92655541001
3947786
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 126 60-140121 4 3020ND25.2 24.2
1,1,1-Trichloroethane ug/L 20 138 60-140130 6 3020ND27.6 26.1
1,1,2,2-Tetrachloroethane ug/L 20 125 60-140121 3 3020ND24.9 24.3
1,1,2-Trichloroethane ug/L 20 130 60-140125 4 3020ND26.0 25.0
1,1-Dichloroethane ug/L 20 129 60-140128 1 3020ND25.8 25.7
1,1-Dichloroethene ug/L M12014460-140140 2 3020ND28.8 28.1
1,1-Dichloropropene ug/L M12014360-140136 5 3020ND28.6 27.2
1,2,3-Trichlorobenzene ug/L 20 131 60-140129 2 3020ND26.2 25.7
1,2,3-Trichloropropane ug/L 20 124 60-140120 4 3020ND24.8 23.9
1,2,4-Trichlorobenzene ug/L 20 131 60-140130 1 3020ND26.2 26.0
1,2,4-Trimethylbenzene ug/L 20 127 60-140124 3 3020ND25.5 24.8
1,2-Dibromo-3-
chloropropane ug/L 20 120 60-140115 4 3020ND24.1 23.1
1,2-Dibromoethane (EDB)ug/L 20 123 60-140122 1 3020ND24.7 24.5
1,2-Dichlorobenzene ug/L 20 122 60-140122 1 3020ND24.5 24.3
1,2-Dichloroethane ug/L 20 139 60-140132 5 3020ND27.8 26.5
1,2-Dichloropropane ug/L 20 136 60-140128 6 3020ND27.2 25.6
1,3,5-Trimethylbenzene ug/L 20 127 60-140122 4 3020ND25.3 24.3
1,3-Dichlorobenzene ug/L 20 124 60-140119 4 3020ND24.8 23.9
1,3-Dichloropropane ug/L 20 126 60-140121 4 3020ND25.1 24.3
1,4-Dichlorobenzene ug/L 20 122 60-140115 6 3020ND24.3 22.9
2,2-Dichloropropane ug/L 20 138 60-140134 3 3020ND27.6 26.8
2-Chlorotoluene ug/L 20 121 60-140121 1 3020ND24.3 24.1
4-Chlorotoluene ug/L 20 126 60-140123 3 3020ND25.2 24.6
Benzene ug/L 20 133 60-140127 5 3020ND26.6 25.4
Bromobenzene ug/L 20 120 60-140117 3 3020ND24.1 23.4
Bromochloromethane ug/L 20 126 60-140122 3 3020ND25.2 24.4
Bromodichloromethane ug/L 20 129 60-140122 6 3020ND25.8 24.4
Bromoform ug/L 20 120 60-140118 2 3020ND24.1 23.6
Bromomethane ug/L 20 110 60-140112 2 3020ND22.0 22.5
Carbon tetrachloride ug/L 20 139 60-140129 7 3020ND27.7 25.8
Chlorobenzene ug/L 20 119 60-140115 4 3020ND23.8 22.9
Chloroethane ug/L 20 122 60-140126 3 3020ND24.4 25.1
Chloroform ug/L 20 130 60-140124 4 3020ND26.0 24.9
Chloromethane ug/L 20 137 60-140137 0 3020ND27.3 27.3
cis-1,2-Dichloroethene ug/L 20 135 60-140131 2 3020ND26.9 26.3
cis-1,3-Dichloropropene ug/L 20 131 60-140125 5 3020ND26.2 25.0
Dibromochloromethane ug/L 20 124 60-140120 3 3020ND24.8 24.0
Dibromomethane ug/L 20 127 60-140119 7 3020ND25.4 23.7
Dichlorodifluoromethane ug/L 20 122 60-140124 2 3020ND24.4 24.9
Diisopropyl ether ug/L 20 133 60-140123 7 3020ND26.5 24.6
Ethylbenzene ug/L 20 122 60-140117 4 3020ND24.4 23.4
Hexachloro-1,3-butadiene ug/L 20 137 60-140139 1 3020ND27.5 27.8
Isopropylbenzene(Cumene)ug/L 20 126 60-140124 1 3020ND25.1 24.9
m&p-Xylene ug/L 40 120 60-140118 2 3040ND48.2 47.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3947785MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92655541001
3947786
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 20 123 60-140115 7 3020ND24.5 23.0
Methylene Chloride ug/L 20 132 60-140132 0 3020ND26.5 26.4
n-Butylbenzene ug/L 20 138 60-140136 1 3020ND27.6 27.2
n-Propylbenzene ug/L 20 127 60-140125 1 3020ND25.3 25.0
Naphthalene ug/L 20 127 60-140124 2 3020ND25.4 24.9
o-Xylene ug/L 20 118 60-140116 2 3020ND23.6 23.2
sec-Butylbenzene ug/L 20 132 60-140129 2 3020ND26.4 25.8
Styrene ug/L 20 123 60-140119 3 3020ND24.5 23.8
tert-Butylbenzene ug/L 20 105 60-140105 0 3020ND21.1 21.0
Tetrachloroethene ug/L 20 118 60-140114 3 3020ND23.6 22.9
Toluene ug/L 20 123 60-140115 7 3020ND24.7 23.0
trans-1,2-Dichloroethene ug/L 20 136 60-140131 4 3020ND27.3 26.3
trans-1,3-Dichloropropene ug/L 20 130 60-140123 6 3020ND26.1 24.6
Trichloroethene ug/L 20 129 60-140122 6 3020ND25.9 24.3
Trichlorofluoromethane ug/L 20 131 60-140127 3 3020ND26.2 25.4
Vinyl chloride ug/L 20 110 60-140109 1 3020ND22.0 21.8
1,2-Dichloroethane-d4 (S)%109 70-130104
4-Bromofluorobenzene (S)%98 70-130102
Toluene-d8 (S)%102 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
759770
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92655319001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3946326
Associated Lab Samples:92655319001
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 03/06/23 18:501.9
1,1,1-Trichloroethane ug/kg ND 5.0 03/06/23 18:502.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 03/06/23 18:501.3
1,1,2-Trichloroethane ug/kg ND 5.0 03/06/23 18:501.7
1,1-Dichloroethane ug/kg ND 5.0 03/06/23 18:502.1
1,1-Dichloroethene ug/kg ND 5.0 03/06/23 18:502.1
1,1-Dichloropropene ug/kg ND 5.0 v103/06/23 18:502.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 03/06/23 18:504.0
1,2,3-Trichloropropane ug/kg ND 5.0 03/06/23 18:502.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 03/06/23 18:504.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 03/06/23 18:503.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 03/06/23 18:501.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 03/06/23 18:502.2
1,2-Dichlorobenzene ug/kg ND 5.0 03/06/23 18:501.8
1,2-Dichloroethane ug/kg ND 5.0 03/06/23 18:503.3
1,2-Dichloropropane ug/kg ND 5.0 03/06/23 18:501.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 03/06/23 18:501.7
1,3-Dichlorobenzene ug/kg ND 5.0 03/06/23 18:501.6
1,3-Dichloropropane ug/kg ND 5.0 03/06/23 18:501.6
1,4-Dichlorobenzene ug/kg ND 5.0 03/06/23 18:501.3
2,2-Dichloropropane ug/kg ND 5.0 03/06/23 18:503.8
2-Butanone (MEK)ug/kg ND 100 03/06/23 18:5024.0
2-Chlorotoluene ug/kg ND 5.0 03/06/23 18:501.8
2-Hexanone ug/kg ND 50.0 03/06/23 18:504.8
4-Chlorotoluene ug/kg ND 5.0 03/06/23 18:502.8
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 03/06/23 18:504.8
Acetone ug/kg ND 100 03/06/23 18:5032.1
Benzene ug/kg ND 5.0 03/06/23 18:502.0
Bromobenzene ug/kg ND 5.0 03/06/23 18:501.6
Bromochloromethane ug/kg ND 5.0 03/06/23 18:501.5
Bromodichloromethane ug/kg ND 5.0 03/06/23 18:501.9
Bromoform ug/kg ND 5.0 03/06/23 18:501.8
Bromomethane ug/kg ND 20.0 03/06/23 18:5015.5
Carbon tetrachloride ug/kg ND 5.0 IK03/06/23 18:501.9
Chlorobenzene ug/kg ND 5.0 03/06/23 18:502.9
Chloroethane ug/kg ND 10.0 03/06/23 18:503.9
Chloroform ug/kg ND 5.0 03/06/23 18:504.2
Chloromethane ug/kg ND 10.0 03/06/23 18:504.2
cis-1,2-Dichloroethene ug/kg ND 5.0 03/06/23 18:501.7
cis-1,3-Dichloropropene ug/kg ND 5.0 03/06/23 18:501.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3946326
Associated Lab Samples:92655319001
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 IK03/06/23 18:502.8
Dibromomethane ug/kg ND 5.0 03/06/23 18:501.1
Dichlorodifluoromethane ug/kg ND 10.0 03/06/23 18:505.1
Diisopropyl ether ug/kg ND 5.0 03/06/23 18:501.4
Ethylbenzene ug/kg ND 5.0 03/06/23 18:502.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 03/06/23 18:508.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 03/06/23 18:501.7
m&p-Xylene ug/kg ND 10.0 03/06/23 18:503.4
Methyl-tert-butyl ether ug/kg ND 5.0 03/06/23 18:501.9
Methylene Chloride ug/kg ND 20.0 03/06/23 18:5013.7
n-Butylbenzene ug/kg ND 5.0 03/06/23 18:503.2
n-Propylbenzene ug/kg ND 5.0 03/06/23 18:501.8
Naphthalene ug/kg ND 5.0 03/06/23 18:502.6
o-Xylene ug/kg ND 5.0 03/06/23 18:502.2
p-Isopropyltoluene ug/kg ND 5.0 03/06/23 18:502.5
sec-Butylbenzene ug/kg ND 5.0 03/06/23 18:502.2
Styrene ug/kg ND 5.0 IK03/06/23 18:501.3
tert-Butylbenzene ug/kg ND 5.0 03/06/23 18:501.8
Tetrachloroethene ug/kg ND 5.0 03/06/23 18:501.6
Toluene ug/kg ND 5.0 03/06/23 18:503.4
trans-1,2-Dichloroethene ug/kg ND 5.0 03/06/23 18:504.2
trans-1,3-Dichloropropene ug/kg ND 5.0 03/06/23 18:501.7
Trichloroethene ug/kg ND 5.0 03/06/23 18:504.0
Trichlorofluoromethane ug/kg ND 5.0 03/06/23 18:502.8
Vinyl acetate ug/kg ND 50.0 03/06/23 18:5010.3
Vinyl chloride ug/kg ND 10.0 03/06/23 18:502.5
Xylene (Total)ug/kg ND 10.0 03/06/23 18:502.8
1,2-Dichloroethane-d4 (S)%108 70-130 03/06/23 18:50
4-Bromofluorobenzene (S)%102 70-130 03/06/23 18:50
Toluene-d8 (S)%102 70-130 03/06/23 18:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3946327LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 456500 91 70-130
1,1,1-Trichloroethane ug/kg 519500 104 70-130
1,1,2,2-Tetrachloroethane ug/kg 486500 97 70-130
1,1,2-Trichloroethane ug/kg 461500 92 70-130
1,1-Dichloroethane ug/kg 524500 105 70-130
1,1-Dichloroethene ug/kg 530500 106 70-130
1,1-Dichloropropene ug/kg 599 v150012070-130
1,2,3-Trichlorobenzene ug/kg 507500 101 70-130
1,2,3-Trichloropropane ug/kg 483500 97 70-130
1,2,4-Trichlorobenzene ug/kg 532500 106 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3946327LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 505500 101 70-130
1,2-Dibromo-3-chloropropane ug/kg 519500 104 67-130
1,2-Dibromoethane (EDB)ug/kg 504500 101 70-130
1,2-Dichlorobenzene ug/kg 502500 100 70-130
1,2-Dichloroethane ug/kg 502500 100 70-130
1,2-Dichloropropane ug/kg 478500 96 70-130
1,3,5-Trimethylbenzene ug/kg 533500 107 70-130
1,3-Dichlorobenzene ug/kg 495500 99 70-130
1,3-Dichloropropane ug/kg 513500 103 70-130
1,4-Dichlorobenzene ug/kg 463500 93 70-130
2,2-Dichloropropane ug/kg 507500 101 67-130
2-Butanone (MEK)ug/kg 10401000 104 66-130
2-Chlorotoluene ug/kg 515500 103 70-130
2-Hexanone ug/kg 9671000 97 70-130
4-Chlorotoluene ug/kg 522500 104 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 9841000 98 70-130
Acetone ug/kg 10501000 105 67-130
Benzene ug/kg 461500 92 70-130
Bromobenzene ug/kg 497500 99 70-130
Bromochloromethane ug/kg 532500 106 70-130
Bromodichloromethane ug/kg 514500 103 70-130
Bromoform ug/kg 485500 97 70-130
Bromomethane ug/kg 389500 78 53-175
Carbon tetrachloride ug/kg 472 IK5009470-130
Chlorobenzene ug/kg 469500 94 70-130
Chloroethane ug/kg 521500 104 70-135
Chloroform ug/kg 490500 98 70-130
Chloromethane ug/kg 549500 110 64-130
cis-1,2-Dichloroethene ug/kg 533500 107 70-130
cis-1,3-Dichloropropene ug/kg 527500 105 70-130
Dibromochloromethane ug/kg 449 IK5009070-130
Dibromomethane ug/kg 472500 94 70-130
Dichlorodifluoromethane ug/kg 576500 115 63-145
Diisopropyl ether ug/kg 517500 103 68-130
Ethylbenzene ug/kg 460500 92 70-130
Hexachloro-1,3-butadiene ug/kg 541500 108 70-130
Isopropylbenzene (Cumene)ug/kg 490500 98 70-130
m&p-Xylene ug/kg 9831000 98 70-130
Methyl-tert-butyl ether ug/kg 502500 100 70-130
Methylene Chloride ug/kg 528500 106 67-130
n-Butylbenzene ug/kg 533500 107 70-130
n-Propylbenzene ug/kg 507500 101 70-130
Naphthalene ug/kg 535500 107 70-130
o-Xylene ug/kg 495500 99 70-130
p-Isopropyltoluene ug/kg 549500 110 70-130
sec-Butylbenzene ug/kg 514500 103 70-130
Styrene ug/kg 530 IK50010670-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3946327LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 538500 108 64-130
Tetrachloroethene ug/kg 508500 102 70-130
Toluene ug/kg 476500 95 70-130
trans-1,2-Dichloroethene ug/kg 540500 108 70-130
trans-1,3-Dichloropropene ug/kg 511500 102 70-130
Trichloroethene ug/kg 514500 103 70-130
Trichlorofluoromethane ug/kg 491500 98 70-130
Vinyl acetate ug/kg 10801000 108 70-134
Vinyl chloride ug/kg 540500 108 68-130
Xylene (Total)ug/kg 14801500 99 70-130
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%107 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3946328MATRIX SPIKE SAMPLE:
MSSpike
Result
92655165001
1,1,1,2-Tetrachloroethane ug/kg 696629 110 58-140ND
1,1,1-Trichloroethane ug/kg 873629 139 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 855629 136 52-139ND
1,1,2-Trichloroethane ug/kg 732629 116 56-140ND
1,1-Dichloroethane ug/kg 862629 137 58-145ND
1,1-Dichloroethene ug/kg 927629 147 57-158ND
1,1-Dichloropropene ug/kg 992 M1,v162915758-151ND
1,2,3-Trichlorobenzene ug/kg 280 M16294448-149ND
1,2,3-Trichloropropane ug/kg 804629 128 54-132ND
1,2,4-Trichlorobenzene ug/kg 525629 83 51-151ND
1,2,4-Trimethylbenzene ug/kg 783629 124 38-170ND
1,2-Dibromo-3-chloropropane ug/kg 563629 89 44-134ND
1,2-Dibromoethane (EDB)ug/kg 751629 119 60-138ND
1,2-Dichlorobenzene ug/kg 782629 124 59-147ND
1,2-Dichloroethane ug/kg 784629 125 57-139ND
1,2-Dichloropropane ug/kg 777629 123 62-145ND
1,3,5-Trimethylbenzene ug/kg 814629 129 47-159ND
1,3-Dichlorobenzene ug/kg 745629 118 58-144ND
1,3-Dichloropropane ug/kg 764629 121 60-142ND
1,4-Dichlorobenzene ug/kg 681629 108 57-143ND
2,2-Dichloropropane ug/kg 782629 124 37-144ND
2-Butanone (MEK)ug/kg 1890 M1126015028-146ND
2-Chlorotoluene ug/kg 788629 125 55-158ND
2-Hexanone ug/kg 14801260 118 44-141ND
4-Chlorotoluene ug/kg 745629 118 55-146ND
4-Methyl-2-pentanone (MIBK)ug/kg 15701260 124 50-138ND
Acetone ug/kg 15401260 122 20-136ND
Benzene ug/kg 749629 119 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3946328MATRIX SPIKE SAMPLE:
MSSpike
Result
92655165001
Bromobenzene ug/kg 726629 115 59-145ND
Bromochloromethane ug/kg 840629 133 57-143ND
Bromodichloromethane ug/kg 789629 125 53-133ND
Bromoform ug/kg 750629 119 48-133ND
Bromomethane ug/kg 502629 80 10-167ND
Carbon tetrachloride ug/kg 596 IK6299557-147ND
Chlorobenzene ug/kg 736629 117 61-144ND
Chloroethane ug/kg 617629 98 10-153ND
Chloroform ug/kg 856629 136 58-141ND
Chloromethane ug/kg 904629 143 54-165ND
cis-1,2-Dichloroethene ug/kg 899629 143 59-144ND
cis-1,3-Dichloropropene ug/kg 811629 129 56-137ND
Dibromochloromethane ug/kg 676 IK62910753-139ND
Dibromomethane ug/kg 723629 115 60-136ND
Dichlorodifluoromethane ug/kg 1150 M162918349-177ND
Diisopropyl ether ug/kg 887 M162914153-136ND
Ethylbenzene ug/kg 721629 115 53-150ND
Hexachloro-1,3-butadiene ug/kg 1220 M162919342-186ND
Isopropylbenzene (Cumene)ug/kg 776629 123 62-154ND
m&p-Xylene ug/kg 15001260 119 49-156ND
Methyl-tert-butyl ether ug/kg 833629 132 54-133ND
Methylene Chloride ug/kg 968 M162915450-153ND
n-Butylbenzene ug/kg 927629 147 44-174ND
n-Propylbenzene ug/kg 776629 123 52-157ND
Naphthalene ug/kg 254629 40 37-150ND
o-Xylene ug/kg 762629 121 54-150ND
p-Isopropyltoluene ug/kg 872629 139 50-164ND
sec-Butylbenzene ug/kg 870629 138 58-161ND
Styrene ug/kg 821 IK62913060-148ND
tert-Butylbenzene ug/kg 805629 128 44-151ND
Tetrachloroethene ug/kg 692629 110 53-151ND
Toluene ug/kg 747629 119 52-148ND
trans-1,2-Dichloroethene ug/kg 888629 141 60-148ND
trans-1,3-Dichloropropene ug/kg 801629 127 55-133ND
Trichloroethene ug/kg 793629 126 60-148ND
Trichlorofluoromethane ug/kg 820629 130 10-154ND
Vinyl acetate ug/kg 15601260 124 50-149ND
Vinyl chloride ug/kg 793629 126 57-157ND
Xylene (Total)ug/kg 22601890 120 52-153ND
1,2-Dichloroethane-d4 (S)%112 70-130
4-Bromofluorobenzene (S)%112 70-130
Toluene-d8 (S)%103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655165002
3946329SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND v130ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND IK30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND IK30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655165002
3946329SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND IK30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%115113
4-Bromofluorobenzene (S)%110113
Toluene-d8 (S)%103102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
760045
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92655319004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3947595
Associated Lab Samples:92655319004
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 03/09/23 10:091.9
1,1,1-Trichloroethane ug/kg ND 5.0 03/09/23 10:092.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 03/09/23 10:091.3
1,1,2-Trichloroethane ug/kg ND 5.0 03/09/23 10:091.7
1,1-Dichloroethane ug/kg ND 5.0 03/09/23 10:092.1
1,1-Dichloroethene ug/kg ND 5.0 03/09/23 10:092.1
1,1-Dichloropropene ug/kg ND 5.0 03/09/23 10:092.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 03/09/23 10:094.0
1,2,3-Trichloropropane ug/kg ND 5.0 03/09/23 10:092.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 03/09/23 10:094.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 03/09/23 10:093.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 03/09/23 10:091.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 03/09/23 10:092.2
1,2-Dichlorobenzene ug/kg ND 5.0 03/09/23 10:091.8
1,2-Dichloroethane ug/kg ND 5.0 03/09/23 10:093.3
1,2-Dichloropropane ug/kg ND 5.0 03/09/23 10:091.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 03/09/23 10:091.7
1,3-Dichlorobenzene ug/kg ND 5.0 03/09/23 10:091.6
1,3-Dichloropropane ug/kg ND 5.0 03/09/23 10:091.6
1,4-Dichlorobenzene ug/kg ND 5.0 03/09/23 10:091.3
2,2-Dichloropropane ug/kg ND 5.0 v203/09/23 10:093.8
2-Butanone (MEK)ug/kg ND 100 03/09/23 10:0924.0
2-Chlorotoluene ug/kg ND 5.0 03/09/23 10:091.8
2-Hexanone ug/kg ND 50.0 v203/09/23 10:094.8
4-Chlorotoluene ug/kg ND 5.0 03/09/23 10:092.8
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 v203/09/23 10:094.8
Acetone ug/kg ND 100 v203/09/23 10:0932.1
Benzene ug/kg ND 5.0 03/09/23 10:092.0
Bromobenzene ug/kg ND 5.0 03/09/23 10:091.6
Bromochloromethane ug/kg ND 5.0 03/09/23 10:091.5
Bromodichloromethane ug/kg ND 5.0 03/09/23 10:091.9
Bromoform ug/kg ND 5.0 03/09/23 10:091.8
Bromomethane ug/kg ND 20.0 v203/09/23 10:0915.5
Carbon tetrachloride ug/kg ND 5.0 IK03/09/23 10:091.9
Chlorobenzene ug/kg ND 5.0 03/09/23 10:092.9
Chloroethane ug/kg ND 10.0 v203/09/23 10:093.9
Chloroform ug/kg ND 5.0 03/09/23 10:094.2
Chloromethane ug/kg ND 10.0 03/09/23 10:094.2
cis-1,2-Dichloroethene ug/kg ND 5.0 03/09/23 10:091.7
cis-1,3-Dichloropropene ug/kg ND 5.0 03/09/23 10:091.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3947595
Associated Lab Samples:92655319004
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 IK03/09/23 10:092.8
Dibromomethane ug/kg ND 5.0 03/09/23 10:091.1
Dichlorodifluoromethane ug/kg ND 10.0 03/09/23 10:095.1
Diisopropyl ether ug/kg ND 5.0 03/09/23 10:091.4
Ethylbenzene ug/kg ND 5.0 03/09/23 10:092.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 03/09/23 10:098.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 03/09/23 10:091.7
m&p-Xylene ug/kg ND 10.0 03/09/23 10:093.4
Methyl-tert-butyl ether ug/kg ND 5.0 03/09/23 10:091.9
Methylene Chloride ug/kg ND 20.0 03/09/23 10:0913.7
n-Butylbenzene ug/kg ND 5.0 03/09/23 10:093.2
n-Propylbenzene ug/kg ND 5.0 03/09/23 10:091.8
Naphthalene ug/kg ND 5.0 03/09/23 10:092.6
o-Xylene ug/kg ND 5.0 03/09/23 10:092.2
p-Isopropyltoluene ug/kg ND 5.0 03/09/23 10:092.5
sec-Butylbenzene ug/kg ND 5.0 03/09/23 10:092.2
Styrene ug/kg ND 5.0 IK03/09/23 10:091.3
tert-Butylbenzene ug/kg ND 5.0 03/09/23 10:091.8
Tetrachloroethene ug/kg ND 5.0 03/09/23 10:091.6
Toluene ug/kg ND 5.0 03/09/23 10:093.4
trans-1,2-Dichloroethene ug/kg ND 5.0 03/09/23 10:094.2
trans-1,3-Dichloropropene ug/kg ND 5.0 03/09/23 10:091.7
Trichloroethene ug/kg ND 5.0 03/09/23 10:094.0
Trichlorofluoromethane ug/kg ND 5.0 03/09/23 10:092.8
Vinyl acetate ug/kg ND 50.0 03/09/23 10:0910.3
Vinyl chloride ug/kg ND 10.0 03/09/23 10:092.5
Xylene (Total)ug/kg ND 10.0 03/09/23 10:092.8
1,2-Dichloroethane-d4 (S)%101 70-130 03/09/23 10:09
4-Bromofluorobenzene (S)%105 70-130 03/09/23 10:09
Toluene-d8 (S)%99 70-130 03/09/23 10:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3947596LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 415500 83 70-130
1,1,1-Trichloroethane ug/kg 462500 92 70-130
1,1,2,2-Tetrachloroethane ug/kg 440500 88 70-130
1,1,2-Trichloroethane ug/kg 429500 86 70-130
1,1-Dichloroethane ug/kg 425500 85 70-130
1,1-Dichloroethene ug/kg 428500 86 70-130
1,1-Dichloropropene ug/kg 489500 98 70-130
1,2,3-Trichlorobenzene ug/kg 459500 92 70-130
1,2,3-Trichloropropane ug/kg 445500 89 70-130
1,2,4-Trichlorobenzene ug/kg 464500 93 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3947596LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 433500 87 70-130
1,2-Dibromo-3-chloropropane ug/kg 436500 87 67-130
1,2-Dibromoethane (EDB)ug/kg 464500 93 70-130
1,2-Dichlorobenzene ug/kg 449500 90 70-130
1,2-Dichloroethane ug/kg 408500 82 70-130
1,2-Dichloropropane ug/kg 408500 82 70-130
1,3,5-Trimethylbenzene ug/kg 455500 91 70-130
1,3-Dichlorobenzene ug/kg 420500 84 70-130
1,3-Dichloropropane ug/kg 431500 86 70-130
1,4-Dichlorobenzene ug/kg 404500 81 70-130
2,2-Dichloropropane ug/kg 397 v35007967-130
2-Butanone (MEK)ug/kg 8621000 86 66-130
2-Chlorotoluene ug/kg 431500 86 70-130
2-Hexanone ug/kg 761 v310007670-130
4-Chlorotoluene ug/kg 444500 89 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 792 v310007970-130
Acetone ug/kg 787 v310007967-130
Benzene ug/kg 411500 82 70-130
Bromobenzene ug/kg 443500 89 70-130
Bromochloromethane ug/kg 491500 98 70-130
Bromodichloromethane ug/kg 455500 91 70-130
Bromoform ug/kg 450500 90 70-130
Bromomethane ug/kg 319 v35006453-175
Carbon tetrachloride ug/kg 404 IK5008170-130
Chlorobenzene ug/kg 429500 86 70-130
Chloroethane ug/kg 394 v35007970-135
Chloroform ug/kg 455500 91 70-130
Chloromethane ug/kg 455500 91 64-130
cis-1,2-Dichloroethene ug/kg 445500 89 70-130
cis-1,3-Dichloropropene ug/kg 456500 91 70-130
Dibromochloromethane ug/kg 413 IK5008370-130
Dibromomethane ug/kg 433500 87 70-130
Dichlorodifluoromethane ug/kg 531500 106 63-145
Diisopropyl ether ug/kg 414500 83 68-130
Ethylbenzene ug/kg 407500 81 70-130
Hexachloro-1,3-butadiene ug/kg 438500 88 70-130
Isopropylbenzene (Cumene)ug/kg 442500 88 70-130
m&p-Xylene ug/kg 8501000 85 70-130
Methyl-tert-butyl ether ug/kg 428500 86 70-130
Methylene Chloride ug/kg 405500 81 67-130
n-Butylbenzene ug/kg 439500 88 70-130
n-Propylbenzene ug/kg 424500 85 70-130
Naphthalene ug/kg 477500 95 70-130
o-Xylene ug/kg 455500 91 70-130
p-Isopropyltoluene ug/kg 461500 92 70-130
sec-Butylbenzene ug/kg 439500 88 70-130
Styrene ug/kg 465 IK5009370-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3947596LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 424500 85 64-130
Tetrachloroethene ug/kg 432500 86 70-130
Toluene ug/kg 414500 83 70-130
trans-1,2-Dichloroethene ug/kg 436500 87 70-130
trans-1,3-Dichloropropene ug/kg 434500 87 70-130
Trichloroethene ug/kg 460500 92 70-130
Trichlorofluoromethane ug/kg 424500 85 70-130
Vinyl acetate ug/kg 8581000 86 70-134
Vinyl chloride ug/kg 416500 83 68-130
Xylene (Total)ug/kg 13001500 87 70-130
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%111 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3947597MATRIX SPIKE SAMPLE:
MSSpike
Result
92655319004
1,1,1,2-Tetrachloroethane ug/kg 627798 79 58-140ND
1,1,1-Trichloroethane ug/kg 799798 100 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 726798 91 52-139ND
1,1,2-Trichloroethane ug/kg 656798 82 56-140ND
1,1-Dichloroethane ug/kg 744798 93 58-145ND
1,1-Dichloroethene ug/kg 797798 100 57-158ND
1,1-Dichloropropene ug/kg 838798 105 58-151ND
1,2,3-Trichlorobenzene ug/kg 218 M17982748-149ND
1,2,3-Trichloropropane ug/kg 659798 82 54-132ND
1,2,4-Trichlorobenzene ug/kg 477798 60 51-151ND
1,2,4-Trimethylbenzene ug/kg 657798 82 38-170ND
1,2-Dibromo-3-chloropropane ug/kg 500798 63 44-134ND
1,2-Dibromoethane (EDB)ug/kg 673798 84 60-138ND
1,2-Dichlorobenzene ug/kg 712798 89 59-147ND
1,2-Dichloroethane ug/kg 678798 85 57-139ND
1,2-Dichloropropane ug/kg 656798 82 62-145ND
1,3,5-Trimethylbenzene ug/kg 702798 88 47-159ND
1,3-Dichlorobenzene ug/kg 664798 83 58-144ND
1,3-Dichloropropane ug/kg 670798 84 60-142ND
1,4-Dichlorobenzene ug/kg 634798 79 57-143ND
2,2-Dichloropropane ug/kg 631 v37987937-144ND
2-Butanone (MEK)ug/kg 11201590 70 28-146ND
2-Chlorotoluene ug/kg 699798 87 55-158ND
2-Hexanone ug/kg 973 v315906144-141ND
4-Chlorotoluene ug/kg 674798 84 55-146ND
4-Methyl-2-pentanone (MIBK)ug/kg 1130 v315907150-138ND
Acetone ug/kg 1010 v315906320-136ND
Benzene ug/kg 667798 83 60-145ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3947597MATRIX SPIKE SAMPLE:
MSSpike
Result
92655319004
Bromobenzene ug/kg 658798 82 59-145ND
Bromochloromethane ug/kg 799798 100 57-143ND
Bromodichloromethane ug/kg 706798 88 53-133ND
Bromoform ug/kg 642798 80 48-133ND
Bromomethane ug/kg 393 v37984910-167ND
Carbon tetrachloride ug/kg 555 IK7987057-147ND
Chlorobenzene ug/kg 655798 82 61-144ND
Chloroethane ug/kg 433 v37985410-153ND
Chloroform ug/kg 749798 94 58-141ND
Chloromethane ug/kg 685798 86 54-165ND
cis-1,2-Dichloroethene ug/kg 761798 95 59-144ND
cis-1,3-Dichloropropene ug/kg 680798 85 56-137ND
Dibromochloromethane ug/kg 601 IK7987553-139ND
Dibromomethane ug/kg 636798 80 60-136ND
Dichlorodifluoromethane ug/kg 883798 111 49-177ND
Diisopropyl ether ug/kg 706798 88 53-136ND
Ethylbenzene ug/kg 633798 79 53-150ND
Hexachloro-1,3-butadiene ug/kg 622798 78 42-186ND
Isopropylbenzene (Cumene)ug/kg 688798 86 62-154ND
m&p-Xylene ug/kg 13101590 82 49-156ND
Methyl-tert-butyl ether ug/kg 716798 90 54-133ND
Methylene Chloride ug/kg 728798 91 50-153ND
n-Butylbenzene ug/kg 675798 85 44-174ND
n-Propylbenzene ug/kg 648798 81 52-157ND
Naphthalene ug/kg 244 M17983137-150ND
o-Xylene ug/kg 700798 88 54-150ND
p-Isopropyltoluene ug/kg 733798 92 50-164ND
sec-Butylbenzene ug/kg 722798 90 58-161ND
Styrene ug/kg 731 IK7989260-148ND
tert-Butylbenzene ug/kg 692798 87 44-151ND
Tetrachloroethene ug/kg 606798 76 53-151ND
Toluene ug/kg 693798 87 52-148ND
trans-1,2-Dichloroethene ug/kg 736798 92 60-148ND
trans-1,3-Dichloropropene ug/kg 659798 83 55-133ND
Trichloroethene ug/kg 683798 86 60-148ND
Trichlorofluoromethane ug/kg 687798 86 10-154ND
Vinyl acetate ug/kg 13301590 83 50-149ND
Vinyl chloride ug/kg 600798 75 57-157ND
Xylene (Total)ug/kg 20102400 84 52-153ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%112 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655502001
3947598SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30<2.9
1,1,1-Trichloroethane ug/kg ND 30<3.9
1,1,2,2-Tetrachloroethane ug/kg ND 30<2.0
1,1,2-Trichloroethane ug/kg ND 30<2.5
1,1-Dichloroethane ug/kg ND 30<3.1
1,1-Dichloroethene ug/kg ND 30<3.1
1,1-Dichloropropene ug/kg ND 30<3.6
1,2,3-Trichlorobenzene ug/kg ND 30<6.1
1,2,3-Trichloropropane ug/kg ND 30<3.8
1,2,4-Trichlorobenzene ug/kg ND 30<6.4
1,2,4-Trimethylbenzene ug/kg ND 30<4.5
1,2-Dibromo-3-chloropropane ug/kg ND 30<2.9
1,2-Dibromoethane (EDB)ug/kg ND 30<3.3
1,2-Dichlorobenzene ug/kg ND 30<2.7
1,2-Dichloroethane ug/kg ND 30<5.0
1,2-Dichloropropane ug/kg ND 30<2.3
1,3,5-Trimethylbenzene ug/kg ND 30<2.5
1,3-Dichlorobenzene ug/kg ND 30<2.4
1,3-Dichloropropane ug/kg ND 30<2.4
1,4-Dichlorobenzene ug/kg 3.8J 30<2.0
2,2-Dichloropropane ug/kg ND v230<5.7
2-Butanone (MEK)ug/kg ND 30<36.4
2-Chlorotoluene ug/kg ND 30<2.7
2-Hexanone ug/kg ND v230<7.3
4-Chlorotoluene ug/kg ND 30<4.2
4-Methyl-2-pentanone (MIBK)ug/kg ND v230<7.3
Acetone ug/kg ND v230<48.7
Benzene ug/kg ND 30<3.0
Bromobenzene ug/kg ND 30<2.5
Bromochloromethane ug/kg ND 30<2.2
Bromodichloromethane ug/kg ND 30<2.9
Bromoform ug/kg ND 30<2.7
Bromomethane ug/kg ND v230<23.5
Carbon tetrachloride ug/kg ND IK30<2.8
Chlorobenzene ug/kg ND 30<4.4
Chloroethane ug/kg ND v230<5.9
Chloroform ug/kg ND 30<6.3
Chloromethane ug/kg ND 30<6.4
cis-1,2-Dichloroethene ug/kg ND 30<2.6
cis-1,3-Dichloropropene ug/kg ND 30<2.1
Dibromochloromethane ug/kg ND IK30<4.3
Dibromomethane ug/kg ND 30<1.6
Dichlorodifluoromethane ug/kg ND 30<7.7
Diisopropyl ether ug/kg ND 30<2.0
Ethylbenzene ug/kg ND 30<3.5
Hexachloro-1,3-butadiene ug/kg ND 30<12.4
Isopropylbenzene (Cumene)ug/kg ND 30<2.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655502001
3947598SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30<5.2
Methyl-tert-butyl ether ug/kg ND 30<2.8
Methylene Chloride ug/kg ND 30<20.8
n-Butylbenzene ug/kg ND 30<4.8
n-Propylbenzene ug/kg ND 30<2.7
Naphthalene ug/kg ND 30<4.0
o-Xylene ug/kg ND 30<3.4
p-Isopropyltoluene ug/kg ND 30<3.7
sec-Butylbenzene ug/kg ND 30<3.3
Styrene ug/kg ND IK30<2.0
tert-Butylbenzene ug/kg ND 30<2.7
Tetrachloroethene ug/kg ND 30<2.4
Toluene ug/kg ND 30<5.2
trans-1,2-Dichloroethene ug/kg ND 30<6.4
trans-1,3-Dichloropropene ug/kg ND 30<2.6
Trichloroethene ug/kg ND 30<6.1
Trichlorofluoromethane ug/kg ND 30<4.2
Vinyl acetate ug/kg ND 30<15.6
Vinyl chloride ug/kg ND 30<3.9
Xylene (Total)ug/kg ND 30<4.3
1,2-Dichloroethane-d4 (S)%10098
4-Bromofluorobenzene (S)%109109
Toluene-d8 (S)%99100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
760330
EPA 625.1
EPA 625.1
625 MSS
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92655319005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3949181
Associated Lab Samples:92655319005
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 5.0 03/09/23 15:361.7
2,2'-Oxybis(1-chloropropane)ug/L ND 5.0 03/09/23 15:361.2
2,4,6-Trichlorophenol ug/L ND 10.0 03/09/23 15:361.6
2,4-Dichlorophenol ug/L ND 5.0 03/09/23 15:361.4
2,4-Dimethylphenol ug/L ND 10.0 03/09/23 15:361.7
2,4-Dinitrophenol ug/L ND 50.0 03/09/23 15:3626.0
2,4-Dinitrotoluene ug/L ND 5.0 03/09/23 15:361.6
2,6-Dinitrotoluene ug/L ND 5.0 03/09/23 15:361.7
2-Chloronaphthalene ug/L ND 5.0 03/09/23 15:361.7
2-Chlorophenol ug/L ND 5.0 03/09/23 15:361.2
2-Nitrophenol ug/L ND 5.0 03/09/23 15:361.4
3,3'-Dichlorobenzidine ug/L ND 10.0 03/09/23 15:368.1
4,6-Dinitro-2-methylphenol ug/L ND 10.0 03/09/23 15:367.8
4-Bromophenylphenyl ether ug/L ND 5.0 03/09/23 15:361.8
4-Chloro-3-methylphenol ug/L ND 5.0 03/09/23 15:363.3
4-Chlorophenylphenyl ether ug/L ND 5.0 03/09/23 15:362.0
4-Nitrophenol ug/L ND 10.0 03/09/23 15:366.6
Acenaphthene ug/L ND 5.0 03/09/23 15:362.0
Acenaphthylene ug/L ND 5.0 03/09/23 15:362.0
Anthracene ug/L ND 5.0 03/09/23 15:362.3
Benzo(a)anthracene ug/L ND 5.0 03/09/23 15:362.7
Benzo(a)pyrene ug/L ND 5.0 03/09/23 15:362.8
Benzo(b)fluoranthene ug/L ND 5.0 03/09/23 15:362.6
Benzo(g,h,i)perylene ug/L ND 5.0 03/09/23 15:362.8
Benzo(k)fluoranthene ug/L ND 5.0 03/09/23 15:362.7
bis(2-Chloroethoxy)methane ug/L ND 10.0 03/09/23 15:361.8
bis(2-Chloroethyl) ether ug/L ND 5.0 03/09/23 15:361.9
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 03/09/23 15:363.7
Butylbenzylphthalate ug/L ND 5.0 03/09/23 15:363.1
Chrysene ug/L ND 5.0 03/09/23 15:362.8
Di-n-butylphthalate ug/L ND 5.0 03/09/23 15:362.2
Di-n-octylphthalate ug/L ND 5.0 03/09/23 15:363.9
Dibenz(a,h)anthracene ug/L ND 5.0 03/09/23 15:363.0
Diethylphthalate ug/L ND 5.0 03/09/23 15:362.0
Dimethylphthalate ug/L ND 5.0 03/09/23 15:362.1
Fluoranthene ug/L ND 5.0 03/09/23 15:362.2
Fluorene ug/L ND 5.0 03/09/23 15:362.1
Hexachloro-1,3-butadiene ug/L ND 5.0 03/09/23 15:361.8
Hexachlorobenzene ug/L ND 5.0 03/09/23 15:362.2
Hexachlorocyclopentadiene ug/L ND 10.0 03/09/23 15:361.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3949181
Associated Lab Samples:92655319005
Matrix:Water
AnalyzedMDL
Hexachloroethane ug/L ND 5.0 03/09/23 15:361.4
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 03/09/23 15:362.9
Isophorone ug/L ND 10.0 03/09/23 15:361.7
N-Nitroso-di-n-propylamine ug/L ND 5.0 03/09/23 15:361.3
N-Nitrosodimethylamine ug/L ND 5.0 03/09/23 15:361.9
N-Nitrosodiphenylamine ug/L ND 10.0 03/09/23 15:363.0
Naphthalene ug/L ND 5.0 03/09/23 15:362.1
Nitrobenzene ug/L ND 5.0 03/09/23 15:361.9
Pentachlorophenol ug/L ND 10.0 03/09/23 15:363.8
Phenanthrene ug/L ND 5.0 03/09/23 15:362.0
Phenol ug/L ND 5.0 03/09/23 15:361.4
Pyrene ug/L ND 5.0 03/09/23 15:362.2
2,4,6-Tribromophenol (S)%104 10-137 03/09/23 15:36
2-Fluorobiphenyl (S)%91 15-120 03/09/23 15:36
2-Fluorophenol (S)%79 10-120 03/09/23 15:36
Nitrobenzene-d5 (S)%103 10-120 03/09/23 15:36
Phenol-d6 (S)%60 10-120 03/09/23 15:36
Terphenyl-d14 (S)%123 11-131 03/09/23 15:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3949182LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 27.450 55 44-142
2,2'-Oxybis(1-chloropropane)ug/L 42.150 84 36-166
2,4,6-Trichlorophenol ug/L 46.150 92 37-144
2,4-Dichlorophenol ug/L 48.150 96 1-191
2,4-Dimethylphenol ug/L 59.150 118 32-119
2,4-Dinitrophenol ug/L 180250 72 1-181
2,4-Dinitrotoluene ug/L 47.650 95 39-139
2,6-Dinitrotoluene ug/L 47.950 96 50-158
2-Chloronaphthalene ug/L 40.150 80 60-118
2-Chlorophenol ug/L 43.450 87 23-134
2-Nitrophenol ug/L 50.250 100 29-182
3,3'-Dichlorobenzidine ug/L 95.6100 96 1-262
4,6-Dinitro-2-methylphenol ug/L 95.6100 96 1-181
4-Bromophenylphenyl ether ug/L 41.950 84 53-127
4-Chloro-3-methylphenol ug/L 84.6100 85 22-147
4-Chlorophenylphenyl ether ug/L 40.250 80 25-158
4-Nitrophenol ug/L 143250 57 1-132
Acenaphthene ug/L 40.350 81 47-145
Acenaphthylene ug/L 41.850 84 33-145
Anthracene ug/L 42.050 84 1-166
Benzo(a)anthracene ug/L 48.850 98 33-143
Benzo(a)pyrene ug/L 48.050 96 17-163
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3949182LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(b)fluoranthene ug/L 50.750 101 24-159
Benzo(g,h,i)perylene ug/L 41.950 84 1-219
Benzo(k)fluoranthene ug/L 49.350 99 11-162
bis(2-Chloroethoxy)methane ug/L 43.150 86 33-184
bis(2-Chloroethyl) ether ug/L 39.850 80 12-158
bis(2-Ethylhexyl)phthalate ug/L 56.450 113 8-158
Butylbenzylphthalate ug/L 57.450 115 1-152
Chrysene ug/L 44.850 90 17-168
Di-n-butylphthalate ug/L 51.750 103 1-118
Di-n-octylphthalate ug/L 59.050 118 4-146
Dibenz(a,h)anthracene ug/L 44.850 90 1-227
Diethylphthalate ug/L 45.150 90 1-114
Dimethylphthalate ug/L 43.950 88 1-112
Fluoranthene ug/L 47.250 94 26-137
Fluorene ug/L 43.150 86 59-121
Hexachloro-1,3-butadiene ug/L 22.350 45 24-116
Hexachlorobenzene ug/L 42.150 84 1-152
Hexachlorocyclopentadiene ug/L 26.350 53 25-150
Hexachloroethane ug/L 23.650 47 40-113
Indeno(1,2,3-cd)pyrene ug/L 44.550 89 1-171
Isophorone ug/L 43.250 86 21-196
N-Nitroso-di-n-propylamine ug/L 43.850 88 1-230
N-Nitrosodimethylamine ug/L 45.350 91 25-150
N-Nitrosodiphenylamine ug/L 44.950 90 25-150
Naphthalene ug/L 33.650 67 21-133
Nitrobenzene ug/L 40.850 82 35-180
Pentachlorophenol ug/L 87.0100 87 14-176
Phenanthrene ug/L 44.250 88 54-120
Phenol ug/L 28.250 56 5-112
Pyrene ug/L 47.450 95 52-115
2,4,6-Tribromophenol (S)%95 10-137
2-Fluorobiphenyl (S)%81 15-120
2-Fluorophenol (S)%66 10-120
Nitrobenzene-d5 (S)%82 10-120
Phenol-d6 (S)%54 10-120
Terphenyl-d14 (S)%93 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3949295MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35783487001
3949296
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L M1,R1507344-14240 57 30501.7U 36.3 20.2
2,2'-Oxybis(1-
chloropropane)ug/L R15013736-16678 55 30501.2U 68.7 39.1
2,4,6-Trichlorophenol ug/L M1502237-1448 30501.6U 10.8 4.0J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3949295MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35783487001
3949296
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4-Dichlorophenol ug/L R150761-19136 70 30501.4U 37.8 18.2
2,4-Dimethylphenol ug/L M1,R15013432-11984 46 30501.7U 66.9 42.0
2,4-Dinitrophenol ug/L M125001-1810 3025026.0U ND ND
2,4-Dinitrotoluene ug/L R15010939-13974 37 30501.6U 54.4 37.2
2,6-Dinitrotoluene ug/L R15011450-15875 41 30501.7U 57.1 37.6
2-Chloronaphthalene ug/L M1,R1509860-11853 59 30501.7U 48.9 26.7
2-Chlorophenol ug/L R1507423-13434 74 30501.2U 36.9 17.1
2-Nitrophenol ug/L R1509429-18236 88 30501.4U 46.9 18.2
3,3'-Dichlorobenzidine ug/L 100 78 1-26268 14 301008.1U 78.0 67.7
4,6-Dinitro-2-methylphenol ug/L M110071-1810 301007.8U ND ND
4-Bromophenylphenyl ether ug/L R15010853-12776 35 30501.8U 54.0 37.8
4-Chloro-3-methylphenol ug/L R110010322-14767 43 301003.3U 103 66.7
4-Chlorophenylphenyl ether ug/L R1509325-15859 46 30502.0U 46.6 29.3
4-Nitrophenol ug/L M125001-1320 302506.6U ND ND
Acenaphthene ug/L R1509647-14559 48 30502.0U 47.9 29.4
Acenaphthylene ug/L R1509733-14560 48 30502.0U 48.6 29.8
Anthracene ug/L R150991-16673 31 30502.3U 49.6 36.3
Benzo(a)anthracene ug/L 50 108 33-14388 20 30502.7U 53.8 44.2
Benzo(a)pyrene ug/L 50 111 17-16384 28 30502.8U 55.5 42.0
Benzo(b)fluoranthene ug/L 50 112 24-15990 22 30502.6U 56.1 44.8
Benzo(g,h,i)perylene ug/L 50 132 1-219102 26 30502.8U 65.9 50.8
Benzo(k)fluoranthene ug/L 50 106 11-16285 22 30502.7U 53.1 42.7
bis(2-
Chloroethoxy)methane ug/L R15010133-18454 60 30501.8U 50.4 27.1
bis(2-Chloroethyl) ether ug/L R15010412-15857 58 30501.9U 52.0 28.7
bis(2-Ethylhexyl)phthalate ug/L 50 126 8-158104 19 30503.7U 63.0 51.9
Butylbenzylphthalate ug/L 50 136 1-152111 21 30503.1U 68.2 55.3
Chrysene ug/L 50 100 17-16886 15 30502.8U 49.9 43.0
Di-n-butylphthalate ug/L 50 113 1-11889 24 30502.2U 56.7 44.5
Di-n-octylphthalate ug/L 50 138 4-146115 18 30503.9U 68.8 57.7
Dibenz(a,h)anthracene ug/L 50 130 1-227101 25 30503.0U 64.9 50.3
Diethylphthalate ug/L R1501011-11471 36 30502.0U 50.7 35.3
Dimethylphthalate ug/L R150991-11266 40 30502.1U 49.7 33.0
Fluoranthene ug/L 50 101 26-13776 28 30502.2U 50.4 37.9
Fluorene ug/L R1509659-12163 41 30502.1U 47.9 31.5
Hexachloro-1,3-butadiene ug/L R1506124-11634 58 30501.8U 30.6 16.8
Hexachlorobenzene ug/L R1501091-15275 37 30502.2U 54.6 37.5
Hexachlorocyclopentadiene ug/L R1507725-15037 69 30501.6U 38.4 18.6
Hexachloroethane ug/L M1,R1505140-11328 58 30501.4U 25.3 13.8
Indeno(1,2,3-cd)pyrene ug/L 50 128 1-17198 26 30502.9U 63.9 49.0
Isophorone ug/L R15010421-19658 56 30501.7U 51.8 29.2
N-Nitroso-di-n-propylamine ug/L R1501001-23057 54 30501.3U 50.1 28.6
N-Nitrosodimethylamine ug/L R1509725-15054 58 30501.9U 48.7 26.9
N-Nitrosodiphenylamine ug/L 50 107 25-15081 27 30503.0U 53.5 40.7
Naphthalene ug/L R1508521-13347 58 30502.1U 42.5 23.4
Nitrobenzene ug/L R1509935-18056 55 30501.9U 49.3 28.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3949295MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35783487001
3949296
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Pentachlorophenol ug/L M1100014-1760 301003.8U ND ND
Phenanthrene ug/L R15010454-12076 32 30502.0U 52.2 37.8
Phenol ug/L R150545-11227 69 30501.4U 27.1 13.3
Pyrene ug/L 50 114 52-11596 17 30502.2U 57.2 48.2
2,4,6-Tribromophenol (S)%36 10-13714
2-Fluorobiphenyl (S)%92 15-12049
2-Fluorophenol (S)%34 10-12012
Nitrobenzene-d5 (S)%95 10-12050
Phenol-d6 (S)%50 10-12024
Terphenyl-d14 (S)%118 11-13192
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
759820
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92655319001, 92655319004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3946426
Associated Lab Samples:92655319001, 92655319004
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 325 03/08/23 08:01128
1,2-Dichlorobenzene ug/kg ND 325 03/08/23 08:01117
1,3-Dichlorobenzene ug/kg ND 325 03/08/23 08:01115
1,4-Dichlorobenzene ug/kg ND 325 03/08/23 08:01124
1-Methylnaphthalene ug/kg ND 325 03/08/23 08:01114
2,2'-Oxybis(1-chloropropane)ug/kg ND 325 03/08/23 08:01154
2,4,5-Trichlorophenol ug/kg ND 325 03/08/23 08:01149
2,4,6-Trichlorophenol ug/kg ND 325 03/08/23 08:01134
2,4-Dichlorophenol ug/kg ND 325 03/08/23 08:01127
2,4-Dimethylphenol ug/kg ND 325 03/08/23 08:01135
2,4-Dinitrophenol ug/kg ND 1620 v103/08/23 08:011000
2,4-Dinitrotoluene ug/kg ND 325 03/08/23 08:01125
2,6-Dinitrotoluene ug/kg ND 325 03/08/23 08:01119
2-Chloronaphthalene ug/kg ND 325 03/08/23 08:01129
2-Chlorophenol ug/kg ND 325 03/08/23 08:01122
2-Methylnaphthalene ug/kg ND 325 03/08/23 08:01130
2-Methylphenol(o-Cresol)ug/kg ND 325 03/08/23 08:01133
2-Nitroaniline ug/kg ND 1620 03/08/23 08:01266
2-Nitrophenol ug/kg ND 325 03/08/23 08:01141
3&4-Methylphenol(m&p Cresol)ug/kg ND 325 03/08/23 08:01131
3,3'-Dichlorobenzidine ug/kg ND 649 03/08/23 08:01219
3-Nitroaniline ug/kg ND 1620 03/08/23 08:01255
4,6-Dinitro-2-methylphenol ug/kg ND 649 v103/08/23 08:01303
4-Bromophenylphenyl ether ug/kg ND 325 03/08/23 08:01125
4-Chloro-3-methylphenol ug/kg ND 649 03/08/23 08:01228
4-Chloroaniline ug/kg ND 649 03/08/23 08:01255
4-Chlorophenylphenyl ether ug/kg ND 325 03/08/23 08:01121
4-Nitroaniline ug/kg ND 649 03/08/23 08:01247
4-Nitrophenol ug/kg ND 1620 03/08/23 08:01628
Acenaphthene ug/kg ND 325 03/08/23 08:01114
Acenaphthylene ug/kg ND 325 03/08/23 08:01114
Aniline ug/kg ND 325 03/08/23 08:01127
Anthracene ug/kg ND 325 03/08/23 08:01106
Benzo(a)anthracene ug/kg ND 325 03/08/23 08:01108
Benzo(a)pyrene ug/kg ND 325 03/08/23 08:01112
Benzo(b)fluoranthene ug/kg ND 325 03/08/23 08:01108
Benzo(g,h,i)perylene ug/kg ND 325 03/08/23 08:01126
Benzo(k)fluoranthene ug/kg ND 325 03/08/23 08:01114
Benzoic Acid ug/kg ND 1620 03/08/23 08:01697
Benzyl alcohol ug/kg ND 649 03/08/23 08:01246
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3946426
Associated Lab Samples:92655319001, 92655319004
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 325 03/08/23 08:01135
bis(2-Chloroethyl) ether ug/kg ND 325 03/08/23 08:01122
bis(2-Ethylhexyl)phthalate ug/kg ND 325 03/08/23 08:01126
Butylbenzylphthalate ug/kg ND 325 03/08/23 08:01137
Chrysene ug/kg ND 325 03/08/23 08:01118
Di-n-butylphthalate ug/kg ND 325 03/08/23 08:01109
Di-n-octylphthalate ug/kg ND 325 03/08/23 08:01128
Dibenz(a,h)anthracene ug/kg ND 325 03/08/23 08:01125
Dibenzofuran ug/kg ND 325 03/08/23 08:01117
Diethylphthalate ug/kg ND 325 03/08/23 08:01119
Dimethylphthalate ug/kg ND 325 03/08/23 08:01118
Fluoranthene ug/kg ND 325 03/08/23 08:01111
Fluorene ug/kg ND 325 03/08/23 08:01114
Hexachloro-1,3-butadiene ug/kg ND 325 03/08/23 08:01141
Hexachlorobenzene ug/kg ND 325 03/08/23 08:01127
Hexachlorocyclopentadiene ug/kg ND 325 03/08/23 08:01186
Hexachloroethane ug/kg ND 325 03/08/23 08:01124
Indeno(1,2,3-cd)pyrene ug/kg ND 325 03/08/23 08:01128
Isophorone ug/kg ND 325 03/08/23 08:01145
N-Nitroso-di-n-propylamine ug/kg ND 325 03/08/23 08:01122
N-Nitrosodimethylamine ug/kg ND 325 03/08/23 08:01109
N-Nitrosodiphenylamine ug/kg ND 325 03/08/23 08:01115
Naphthalene ug/kg ND 325 03/08/23 08:01110
Nitrobenzene ug/kg ND 325 03/08/23 08:01150
Pentachlorophenol ug/kg ND 649 03/08/23 08:01318
Phenanthrene ug/kg ND 325 03/08/23 08:01106
Phenol ug/kg ND 325 03/08/23 08:01145
Pyrene ug/kg ND 325 03/08/23 08:01132
Pyridine ug/kg ND 325 03/08/23 08:01102
2,4,6-Tribromophenol (S)%63 10-131 03/08/23 08:01
2-Fluorobiphenyl (S)%55 10-130 03/08/23 08:01
2-Fluorophenol (S)%53 10-130 03/08/23 08:01
Nitrobenzene-d5 (S)%56 10-130 03/08/23 08:01
Phenol-d6 (S)%55 10-130 03/08/23 08:01
Terphenyl-d14 (S)%59 10-130 03/08/23 08:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3946427LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 12101670 73 43-130
1,2-Dichlorobenzene ug/kg 12101670 73 43-130
1,3-Dichlorobenzene ug/kg 12001670 72 43-130
1,4-Dichlorobenzene ug/kg 11901670 71 44-130
1-Methylnaphthalene ug/kg 12501670 75 47-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3946427LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 13201670 79 29-130
2,4,5-Trichlorophenol ug/kg 13001670 78 47-130
2,4,6-Trichlorophenol ug/kg 13401670 80 47-130
2,4-Dichlorophenol ug/kg 12101670 73 45-130
2,4-Dimethylphenol ug/kg 16601670 100 45-130
2,4-Dinitrophenol ug/kg 7660 v183309227-140
2,4-Dinitrotoluene ug/kg 13601670 82 46-130
2,6-Dinitrotoluene ug/kg 13801670 83 48-130
2-Chloronaphthalene ug/kg 13201670 79 46-130
2-Chlorophenol ug/kg 12201670 73 43-130
2-Methylnaphthalene ug/kg 12301670 74 47-130
2-Methylphenol(o-Cresol)ug/kg 13201670 79 42-130
2-Nitroaniline ug/kg 28203330 84 41-130
2-Nitrophenol ug/kg 12301670 74 48-130
3&4-Methylphenol(m&p Cresol)ug/kg 13501670 81 39-130
3,3'-Dichlorobenzidine ug/kg 22903330 69 41-130
3-Nitroaniline ug/kg 24103330 72 37-130
4,6-Dinitro-2-methylphenol ug/kg 3140 v133309438-141
4-Bromophenylphenyl ether ug/kg 13501670 81 47-130
4-Chloro-3-methylphenol ug/kg 25003330 75 44-130
4-Chloroaniline ug/kg 23803330 71 41-130
4-Chlorophenylphenyl ether ug/kg 12901670 77 45-130
4-Nitroaniline ug/kg 26703330 80 42-130
4-Nitrophenol ug/kg 63208330 76 39-131
Acenaphthene ug/kg 13201670 79 49-130
Acenaphthylene ug/kg 13101670 79 50-130
Aniline ug/kg 10901670 66 38-130
Anthracene ug/kg 12301670 74 49-130
Benzo(a)anthracene ug/kg 12901670 77 51-130
Benzo(a)pyrene ug/kg 11301670 68 51-130
Benzo(b)fluoranthene ug/kg 11501670 69 49-130
Benzo(g,h,i)perylene ug/kg 12001670 72 48-140
Benzo(k)fluoranthene ug/kg 11401670 68 51-130
Benzoic Acid ug/kg 47008330 56 22-130
Benzyl alcohol ug/kg 25703330 77 43-130
bis(2-Chloroethoxy)methane ug/kg 11801670 71 43-130
bis(2-Chloroethyl) ether ug/kg 11901670 71 42-130
bis(2-Ethylhexyl)phthalate ug/kg 13501670 81 43-130
Butylbenzylphthalate ug/kg 13701670 82 44-131
Chrysene ug/kg 13301670 80 51-130
Di-n-butylphthalate ug/kg 13201670 79 46-130
Di-n-octylphthalate ug/kg 13701670 82 45-130
Dibenz(a,h)anthracene ug/kg 11501670 69 48-130
Dibenzofuran ug/kg 13301670 80 10-130
Diethylphthalate ug/kg 12901670 77 48-130
Dimethylphthalate ug/kg 12801670 77 48-130
Fluoranthene ug/kg 13201670 79 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3946427LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 13301670 80 48-130
Hexachloro-1,3-butadiene ug/kg 11401670 68 39-130
Hexachlorobenzene ug/kg 12801670 77 47-130
Hexachlorocyclopentadiene ug/kg 10601670 64 17-130
Hexachloroethane ug/kg 12301670 74 40-130
Indeno(1,2,3-cd)pyrene ug/kg 12001670 72 50-130
Isophorone ug/kg 12501670 75 41-130
N-Nitroso-di-n-propylamine ug/kg 13501670 81 36-130
N-Nitrosodimethylamine ug/kg 11301670 68 34-130
N-Nitrosodiphenylamine ug/kg 13301670 80 48-130
Naphthalene ug/kg 12001670 72 46-130
Nitrobenzene ug/kg 12401670 74 39-130
Pentachlorophenol ug/kg 21403330 64 42-130
Phenanthrene ug/kg 13701670 82 50-130
Phenol ug/kg 12301670 74 42-130
Pyrene ug/kg 13801670 83 50-130
Pyridine ug/kg 10201670 61 26-130
2,4,6-Tribromophenol (S)%77 10-131
2-Fluorobiphenyl (S)%70 10-130
2-Fluorophenol (S)%68 10-130
Nitrobenzene-d5 (S)%67 10-130
Phenol-d6 (S)%70 10-130
Terphenyl-d14 (S)%74 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3946428MATRIX SPIKE SAMPLE:
MSSpike
Result
92655002001
1,2,4-Trichlorobenzene ug/kg 12302100 58 16-130ND
1,2-Dichlorobenzene ug/kg 12202100 58 19-130ND
1,3-Dichlorobenzene ug/kg 11902100 56 19-130ND
1,4-Dichlorobenzene ug/kg 11702100 55 20-130ND
1-Methylnaphthalene ug/kg 12902100 61 19-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 13402100 63 10-130ND
2,4,5-Trichlorophenol ug/kg 13802100 66 19-130ND
2,4,6-Trichlorophenol ug/kg 13802100 65 18-130ND
2,4-Dichlorophenol ug/kg 13402100 64 16-130ND
2,4-Dimethylphenol ug/kg 12302100 58 10-130ND
2,4-Dinitrophenol ug/kg 8300 v1105007910-143ND
2,4-Dinitrotoluene ug/kg 14502100 69 19-130ND
2,6-Dinitrotoluene ug/kg 14402100 68 22-130ND
2-Chloronaphthalene ug/kg 13402100 64 18-130ND
2-Chlorophenol ug/kg 12402100 59 20-130ND
2-Methylnaphthalene ug/kg 12802100 61 18-130ND
2-Methylphenol(o-Cresol)ug/kg 12602100 60 13-130ND
2-Nitroaniline ug/kg 30104220 71 18-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3946428MATRIX SPIKE SAMPLE:
MSSpike
Result
92655002001
2-Nitrophenol ug/kg 13402100 64 19-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 13002100 62 13-130ND
3,3'-Dichlorobenzidine ug/kg 19204220 46 10-130ND
3-Nitroaniline ug/kg 25004220 59 22-130ND
4,6-Dinitro-2-methylphenol ug/kg 3440 v142208210-144ND
4-Bromophenylphenyl ether ug/kg 13402100 63 18-130ND
4-Chloro-3-methylphenol ug/kg 27904220 66 16-130ND
4-Chloroaniline ug/kg 23904220 57 17-130ND
4-Chlorophenylphenyl ether ug/kg 12902100 61 17-130ND
4-Nitroaniline ug/kg 28104220 67 21-130ND
4-Nitrophenol ug/kg 645010500 61 13-131ND
Acenaphthene ug/kg 13402100 63 20-130ND
Acenaphthylene ug/kg 13302100 63 21-130ND
Aniline ug/kg 6252100 30 10-130ND
Anthracene ug/kg 12302100 58 19-130ND
Benzo(a)anthracene ug/kg 12502100 59 17-130ND
Benzo(a)pyrene ug/kg 11102100 53 14-130ND
Benzo(b)fluoranthene ug/kg 11002100 52 11-134ND
Benzo(g,h,i)perylene ug/kg 12202100 58 12-130ND
Benzo(k)fluoranthene ug/kg 11002100 52 15-130ND
Benzoic Acid ug/kg 716010500 68 10-130ND
Benzyl alcohol ug/kg 26404220 63 20-130ND
bis(2-Chloroethoxy)methane ug/kg 12802100 61 16-130ND
bis(2-Chloroethyl) ether ug/kg 11902100 56 18-130ND
bis(2-Ethylhexyl)phthalate ug/kg 13102100 62 11-130ND
Butylbenzylphthalate ug/kg 12702100 60 10-130ND
Chrysene ug/kg 13102100 62 17-130ND
Di-n-butylphthalate ug/kg 13102100 62 16-130ND
Di-n-octylphthalate ug/kg 13302100 63 16-130ND
Dibenz(a,h)anthracene ug/kg 12302100 58 13-130ND
Dibenzofuran ug/kg 14002100 66 19-130ND
Diethylphthalate ug/kg 13702100 65 22-130ND
Dimethylphthalate ug/kg 13802100 65 23-130ND
Fluoranthene ug/kg 13102100 62 14-130ND
Fluorene ug/kg 13702100 65 19-130ND
Hexachloro-1,3-butadiene ug/kg 11102100 53 12-130ND
Hexachlorobenzene ug/kg 12902100 61 17-130ND
Hexachlorocyclopentadiene ug/kg 9612100 46 10-130ND
Hexachloroethane ug/kg 11902100 56 14-130ND
Indeno(1,2,3-cd)pyrene ug/kg 12702100 60 13-130ND
Isophorone ug/kg 13802100 65 17-130ND
N-Nitroso-di-n-propylamine ug/kg 14202100 67 10-130ND
N-Nitrosodimethylamine ug/kg 10502100 50 16-130ND
N-Nitrosodiphenylamine ug/kg 13302100 63 19-130ND
Naphthalene ug/kg 12702100 60 18-130ND
Nitrobenzene ug/kg 12902100 61 15-130ND
Pentachlorophenol ug/kg 25504220 60 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3946428MATRIX SPIKE SAMPLE:
MSSpike
Result
92655002001
Phenanthrene ug/kg 14002100 66 17-130ND
Phenol ug/kg 12102100 58 15-130ND
Pyrene ug/kg 12902100 61 31-130ND
Pyridine ug/kg 5762100 27 10-130ND
2,4,6-Tribromophenol (S)%57 10-131
2-Fluorobiphenyl (S)%52 10-130
2-Fluorophenol (S)%48 10-130
Nitrobenzene-d5 (S)%53 10-130
Phenol-d6 (S)%51 10-130
Terphenyl-d14 (S)%50 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92654931001
3946429SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30160U
1,2-Dichlorobenzene ug/kg ND 30147U
1,3-Dichlorobenzene ug/kg ND 30144U
1,4-Dichlorobenzene ug/kg ND 30155U
1-Methylnaphthalene ug/kg ND 30143U
2,2'-Oxybis(1-chloropropane)ug/kg ND 30194U
2,4,5-Trichlorophenol ug/kg ND 30186U
2,4,6-Trichlorophenol ug/kg ND 30168U
2,4-Dichlorophenol ug/kg ND 30159U
2,4-Dimethylphenol ug/kg ND 30169U
2,4-Dinitrophenol ug/kg ND v1301260U
2,4-Dinitrotoluene ug/kg ND 30157U
2,6-Dinitrotoluene ug/kg ND 30149U
2-Chloronaphthalene ug/kg ND 30162U
2-Chlorophenol ug/kg ND 30153U
2-Methylnaphthalene ug/kg ND 30163U
2-Methylphenol(o-Cresol)ug/kg ND 30167U
2-Nitroaniline ug/kg ND 30333U
2-Nitrophenol ug/kg ND 30176U
3&4-Methylphenol(m&p Cresol)ug/kg ND 30164U
3,3'-Dichlorobenzidine ug/kg ND 30275U
3-Nitroaniline ug/kg ND 30320U
4,6-Dinitro-2-methylphenol ug/kg ND v130380U
4-Bromophenylphenyl ether ug/kg ND 30157U
4-Chloro-3-methylphenol ug/kg ND 30286U
4-Chloroaniline ug/kg ND 30320U
4-Chlorophenylphenyl ether ug/kg ND 30152U
4-Nitroaniline ug/kg ND 30310U
4-Nitrophenol ug/kg ND 30787U
Acenaphthene ug/kg ND 30143U
Acenaphthylene ug/kg ND 30143U
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92654931001
3946429SAMPLE DUPLICATE:
Aniline ug/kg ND 30159U
Anthracene ug/kg ND 30133U
Benzo(a)anthracene ug/kg ND 30136U
Benzo(a)pyrene ug/kg ND 30141U
Benzo(b)fluoranthene ug/kg ND 30136U
Benzo(g,h,i)perylene ug/kg ND 30158U
Benzo(k)fluoranthene ug/kg ND 30143U
Benzoic Acid ug/kg ND 30875U
Benzyl alcohol ug/kg ND 30308U
bis(2-Chloroethoxy)methane ug/kg ND 30169U
bis(2-Chloroethyl) ether ug/kg ND 30153U
bis(2-Ethylhexyl)phthalate ug/kg ND 30158U
Butylbenzylphthalate ug/kg ND 30172U
Chrysene ug/kg ND 30148U
Di-n-butylphthalate ug/kg ND 30137U
Di-n-octylphthalate ug/kg ND 30160U
Dibenz(a,h)anthracene ug/kg ND 30157U
Dibenzofuran ug/kg ND 30147U
Diethylphthalate ug/kg ND 30149U
Dimethylphthalate ug/kg ND 30148U
Fluoranthene ug/kg ND 30139U
Fluorene ug/kg ND 30143U
Hexachloro-1,3-butadiene ug/kg ND 30176U
Hexachlorobenzene ug/kg ND 30159U
Hexachlorocyclopentadiene ug/kg ND 30233U
Hexachloroethane ug/kg ND 30155U
Indeno(1,2,3-cd)pyrene ug/kg ND 30160U
Isophorone ug/kg ND 30181U
N-Nitroso-di-n-propylamine ug/kg ND 30153U
N-Nitrosodimethylamine ug/kg ND 30137U
N-Nitrosodiphenylamine ug/kg ND 30144U
Naphthalene ug/kg ND 30138U
Nitrobenzene ug/kg ND 30189U
Pentachlorophenol ug/kg ND 30399U
Phenanthrene ug/kg ND 30133U
Phenol ug/kg ND 30181U
Pyrene ug/kg ND 30165U
Pyridine ug/kg ND 30128U
2,4,6-Tribromophenol (S)%5458
2-Fluorobiphenyl (S)%5152
2-Fluorophenol (S)%4553
Nitrobenzene-d5 (S)%6064
Phenol-d6 (S)%4857
Terphenyl-d14 (S)%5256
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
759948
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92655319001, 92655319002, 92655319003, 92655319004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3947117
Associated Lab Samples:92655319001, 92655319002, 92655319003, 92655319004
Matrix:Solid
AnalyzedMDL
Aliphatic (C09-C18)mg/kg ND 10.1 N203/10/23 10:2410.1
Aliphatic (C19-C36)mg/kg ND 10.1 N203/10/23 10:2410.1
Aromatic (C11-C22)mg/kg ND 10.1 N203/10/23 10:2410.1
1-Chlorooctadecane (S)%66 40-140 03/10/23 10:24
2-Bromonaphthalene (S)%85 40-140 03/10/23 10:24
2-Fluorobiphenyl (S)%84 40-140 03/10/23 10:24
o-Terphenyl (S)%84 40-140 03/10/23 10:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3947118LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3947119
Aliphatic (C09-C18)mg/kg ND N2104140-14050ND 50
Aliphatic (C19-C36)mg/kg 10.1 N213.3 76 40-1408811.6 14 50
Aromatic (C11-C22)mg/kg 22.4 N228.2 79 40-1407019.6 13 50
1-Chlorooctadecane (S)%74 40-14083
2-Bromonaphthalene (S)%75 40-14065
2-Fluorobiphenyl (S)%76 40-14067
o-Terphenyl (S)%78 40-14063
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
759985
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92655319005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3947277
Associated Lab Samples:92655319005
Matrix:Water
AnalyzedMDL
Aliphatic (C09-C18)ug/L ND 100 N203/08/23 17:10100
Aliphatic (C19-C36)ug/L ND 100 N203/08/23 17:10100
Aromatic (C11-C22)ug/L ND 100 N203/08/23 17:10100
1-Chlorooctadecane (S)%73 40-140 03/08/23 17:10
2-Bromonaphthalene (S)%111 40-140 03/08/23 17:10
2-Fluorobiphenyl (S)%111 40-140 03/08/23 17:10
o-Terphenyl (S)%93 40-140 03/08/23 17:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3947278LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3947279
Aliphatic (C09-C18)ug/L 182 N23006140-14060179 2 50
Aliphatic (C19-C36)ug/L 395 N24009940-14092367 8 50
Aromatic (C11-C22)ug/L 714 N28508440-14085726 2 50
1-Chlorooctadecane (S)%81 40-14074
2-Bromonaphthalene (S)%92 40-14099
2-Fluorobiphenyl (S)%89 40-14096
o-Terphenyl (S)%83 40-14086
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
759747
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92655319001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655291007
3946277SAMPLE DUPLICATE:
Percent Moisture %22.7 N232523.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655319001
3946278SAMPLE DUPLICATE:
Percent Moisture %18.1 N232518.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92655319
NST .001-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
759974
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92655319002, 92655319003, 92655319004
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92655315001
3947240SAMPLE DUPLICATE:
Percent Moisture %23.3 N212523.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
50338862001
3947241SAMPLE DUPLICATE:
Percent Moisture %9.1 N2182510.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 83
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92655319
NST .001-002
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The reported TIC has an 85% or higher match on a mass spectral library search.N
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
Surrogate recovery not evaluated against control limits due to sample dilution.S4
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 83
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92655319
NST .001-002
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92655319001 759948 760623SB-3A (0-2)MADEP EPH MADEP EPH
92655319002 759948 760623SB-3A (7-9)MADEP EPH MADEP EPH
92655319003 759948 760623SB-3A (14-16)MADEP EPH MADEP EPH
92655319004 759948 760623SB-3A (21-23)MADEP EPH MADEP EPH
92655319005 759985 760250TMW-2A MADEP EPH MADEP EPH
92655319005 760673 760741TMW-2A EPA 3010A EPA 6020B
92655319001 870506 870624SB-3A (0-2)EPA 3050B EPA 6020B
92655319004 870506 870624SB-3A (21-23)EPA 3050B EPA 6020B
92655319005 760330 760511TMW-2A EPA 625.1 EPA 625.1
92655319001 759820 760068SB-3A (0-2)EPA 3546 EPA 8270E
92655319004 759820 760068SB-3A (21-23)EPA 3546 EPA 8270E
92655319005 760113TMW-2A SM 6200B
92655319001 759770 760009SB-3A (0-2)EPA 5035A/5030B EPA 8260D
92655319004 760045 760408SB-3A (21-23)EPA 5035A/5030B EPA 8260D
92655319001 759747SB-3A (0-2)SW-846
92655319002 759974SB-3A (7-9)SW-846
92655319003 759974SB-3A (14-16)SW-846
92655319004 759974SB-3A (21-23)SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/15/2023 06:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 83
Page 58 of 83
Page 59 of 83
Page 60 of 83
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
March 15, 2023
Taylor Cannon
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Project Location: NST .001-002
Client Job Number:
Project Number: 92655319
Laboratory Work Order Number: 23C0864
Enclosed are results of analyses for samples as received by the laboratory on March 8, 2023. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Rebecca Faust
Project Manager
Page 1 of 23
Table of Contents
Page 61 of 83
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
23C0864-01 5
23C0864-02 7
23C0864-03 9
23C0864-04 11
23C0864-05 13
Sample Preparation Information 14
QC Data 15
Petroleum Hydrocarbons Analyses - VPH 15
B333760 15
B333896 16
Flag/Qualifier Summary 18
Certifications 19
Chain of Custody/Sample Receipt 20
Page 2 of 23
Table of Contents
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
3/15/2023
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
ATTN: Taylor Cannon
92655319
23C0864
The results of analyses performed on the following samples submitted to CON-TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
NST .001-002
SB-3A (0-2)23C0864-01 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SB-3A (7-9)23C0864-02 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SB-3A (14-16)23C0864-03 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SB-3A (21-23)23C0864-04 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
TMW-2A 23C0864-05 Water MADEP-VPH-Feb
2018 Rev 2.1
[TOC_1]Sample Summary[TOC]
Page 3 of 23
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH, only hydrocarbon ranges were requested and reported.
[TOC_1]Case Narrative[TOC]
MADEP-VPH-Feb 2018 Rev 2.1
Qualifications:
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
2-Methylpentane
B333760-BSD1
Elevated reporting limit due to high concentration of target compounds. MA CAM reporting limit not met.
Analyte & Samples(s) Qualified:
RL-05
C5-C8 Aliphatics
23C0864-01[SB-3A (0-2)]
Unadjusted C5-C8 Aliphatics
23C0864-01[SB-3A (0-2)]
Surrogate recovery outside of control limits due to suspected sample matrix interference. Chromatogram(s) is attached.
Analyte & Samples(s) Qualified:
S-15
2,5-Dibromotoluene (FID)
23C0864-01[SB-3A (0-2)]
2,5-Dibromotoluene (PID)
23C0864-01[SB-3A (0-2)]
MADEP-VPH-Feb 2018 Rev 2.1
No significant modifications were made to the method. All VPH samples were received preserved properly at pH <2 in the proper containers as specified on the chain-of-custody
form unless specified in this narrative.
No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely
covered by methanol in the proper containers specified on the chain-of-custody form unless specified in this narrative.
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Meghan E. Kelley
Reporting Specialist
Page 4 of 23
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/8/2023
Work Order: 23C0864Sample Description:Project Location: NST .001-002
Sample ID: 23C0864-01
Field Sample #: SB-3A (0-2)
Sample Matrix: Soil
Sampled: 3/6/2023 13:45
[TOC_2]23C0864-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.04
Petroleum Hydrocarbons Analyses - VPH
ND 28 3/10/23 8:41 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
2 RL-05Unadjusted C5-C8 Aliphatics
ND 28 3/10/23 8:41 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
2 RL-05C5-C8 Aliphatics
250 28 3/10/23 8:41 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
2Unadjusted C9-C12 Aliphatics
120 28 3/10/23 8:41 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
2C9-C12 Aliphatics
130 28 3/10/23 8:41 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
2C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)207 3/10/23 8:41*S-1570-130
2,5-Dibromotoluene (PID)207 3/10/23 8:41*S-1570-130
[TOC_1]Sample Results[TOC]
Page 5 of 23
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Date Received: 3/8/2023
Work Order: 23C0864Sample Description:Project Location: NST .001-002
Sample ID: 23C0864-01
Field Sample #: SB-3A (0-2)
Sample Matrix: Soil
Sampled: 3/6/2023 13:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
81.6 3/9/23 6:49 WDC% Wt 3/9/23SM 2540G1% Solids
Page 6 of 23
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Date Received: 3/8/2023
Work Order: 23C0864Sample Description:Project Location: NST .001-002
Sample ID: 23C0864-02
Field Sample #: SB-3A (7-9)
Sample Matrix: Soil
Sampled: 3/6/2023 13:55
[TOC_2]23C0864-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.02
Petroleum Hydrocarbons Analyses - VPH
ND 14 3/9/23 15:40 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 14 3/9/23 15:40 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 14 3/9/23 15:40 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 14 3/9/23 15:40 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 14 3/9/23 15:40 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)96.8 3/9/23 15:4070-130
2,5-Dibromotoluene (PID)96.9 3/9/23 15:4070-130
Page 7 of 23
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Date Received: 3/8/2023
Work Order: 23C0864Sample Description:Project Location: NST .001-002
Sample ID: 23C0864-02
Field Sample #: SB-3A (7-9)
Sample Matrix: Soil
Sampled: 3/6/2023 13:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
83.7 3/9/23 6:49 WDC% Wt 3/9/23SM 2540G1% Solids
Page 8 of 23
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Date Received: 3/8/2023
Work Order: 23C0864Sample Description:Project Location: NST .001-002
Sample ID: 23C0864-03
Field Sample #: SB-3A (14-16)
Sample Matrix: Soil
Sampled: 3/6/2023 14:05
[TOC_2]23C0864-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.07
Petroleum Hydrocarbons Analyses - VPH
ND 14 3/9/23 16:10 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 14 3/9/23 16:10 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 14 3/9/23 16:10 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 14 3/9/23 16:10 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 14 3/9/23 16:10 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)97.4 3/9/23 16:1070-130
2,5-Dibromotoluene (PID)97.2 3/9/23 16:1070-130
Page 9 of 23
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Date Received: 3/8/2023
Work Order: 23C0864Sample Description:Project Location: NST .001-002
Sample ID: 23C0864-03
Field Sample #: SB-3A (14-16)
Sample Matrix: Soil
Sampled: 3/6/2023 14:05
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
79.8 3/9/23 6:49 WDC% Wt 3/9/23SM 2540G1% Solids
Page 10 of 23
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Date Received: 3/8/2023
Work Order: 23C0864Sample Description:Project Location: NST .001-002
Sample ID: 23C0864-04
Field Sample #: SB-3A (21-23)
Sample Matrix: Soil
Sampled: 3/6/2023 14:15
[TOC_2]23C0864-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.07
Petroleum Hydrocarbons Analyses - VPH
ND 13 3/9/23 16:39 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 13 3/9/23 16:39 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 13 3/9/23 16:39 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 13 3/9/23 16:39 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 13 3/9/23 16:39 EEHmg/Kg dry 3/9/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)91.3 3/9/23 16:3970-130
2,5-Dibromotoluene (PID)89.9 3/9/23 16:3970-130
Page 11 of 23
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Date Received: 3/8/2023
Work Order: 23C0864Sample Description:Project Location: NST .001-002
Sample ID: 23C0864-04
Field Sample #: SB-3A (21-23)
Sample Matrix: Soil
Sampled: 3/6/2023 14:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
82.4 3/9/23 6:49 WDC% Wt 3/9/23SM 2540G1% Solids
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Date Received: 3/8/2023
Work Order: 23C0864Sample Description:Project Location: NST .001-002
Sample ID: 23C0864-05
Field Sample #: TMW-2A
Sample Matrix: Water
Sampled: 3/6/2023 12:55
[TOC_2]23C0864-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 3/10/23 14:16 EEHg/L 3/10/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 100 3/10/23 14:16 EEHg/L 3/10/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 100 3/10/23 14:16 EEHg/L 3/10/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 100 3/10/23 14:16 EEHg/L 3/10/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 100 3/10/23 14:16 EEHg/L 3/10/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)115 3/10/23 14:1670-130
2,5-Dibromotoluene (PID)117 3/10/23 14:1670-130
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Sample Extraction Data
Prep Method: MA VPH Analytical Method: MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B333760 03/09/2310.4 11.923C0864-01 [SB-3A (0-2)]
B333760 03/09/2310.2 11.723C0864-02 [SB-3A (7-9)]
B333760 03/09/2310.7 12.223C0864-03 [SB-3A (14-16)]
B333760 03/09/2310.7 11.923C0864-04 [SB-3A (21-23)]
Prep Method: MA VPH Analytical Method: MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B333896 03/10/235 5.0023C0864-05 [TMW-2A]
Prep Method: % Solids Analytical Method: SM 2540G
Lab Number [Field ID]Batch Date
B333717 03/09/2323C0864-01 [SB-3A (0-2)]
B333717 03/09/2323C0864-02 [SB-3A (7-9)]
B333717 03/09/2323C0864-03 [SB-3A (14-16)]
B333717 03/09/2323C0864-04 [SB-3A (21-23)]
[TOC_1]Sample Preparation Information[TOC]
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B333760 - MA VPH
[TOC_3]B333760[TOC]
Blank (B333760-BLK1) Prepared & Analyzed: 03/09/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10ND
C5-C8 Aliphatics mg/Kg wet10ND
Unadjusted C9-C12 Aliphatics mg/Kg wet10ND
C9-C12 Aliphatics mg/Kg wet10ND
C9-C10 Aromatics mg/Kg wet10ND
Benzene mg/Kg wet0.050ND
Butylcyclohexane mg/Kg wet0.050ND
Decane mg/Kg wet0.050ND
Ethylbenzene mg/Kg wet0.050ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050ND
2-Methylpentane mg/Kg wet0.050ND
Naphthalene mg/Kg wet0.50ND
Nonane mg/Kg wet0.050ND
Pentane mg/Kg wet0.050ND
Toluene mg/Kg wet0.050ND
1,2,4-Trimethylbenzene mg/Kg wet0.050ND
2,2,4-Trimethylpentane mg/Kg wet0.050ND
m+p Xylene mg/Kg wet0.10ND
o-Xylene mg/Kg wet0.050ND
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)10040.0
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)97.138.8
LCS (B333760-BS1) Prepared & Analyzed: 03/09/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10 7.50 70-1301198.90
Unadjusted C9-C12 Aliphatics mg/Kg wet10 7.50 70-1301108.22
C9-C10 Aromatics mg/Kg wet10 2.50 70-1301112.78
Benzene mg/Kg wet0.050 2.50 70-1301172.94
Butylcyclohexane mg/Kg wet0.050 2.50 70-1301172.92
Decane mg/Kg wet0.050 2.50 70-13093.92.35
Ethylbenzene mg/Kg wet0.050 2.50 70-1301142.86
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050 2.50 70-1301112.76
2-Methylpentane mg/Kg wet0.050 2.50 70-1301253.13
Naphthalene mg/Kg wet0.50 2.50 70-13083.02.07
Nonane mg/Kg wet0.050 2.50 30-1301182.95
Pentane mg/Kg wet0.050 2.50 70-1301202.99
Toluene mg/Kg wet0.050 2.50 70-1301152.87
1,2,4-Trimethylbenzene mg/Kg wet0.050 2.50 70-1301112.78
2,2,4-Trimethylpentane mg/Kg wet0.050 2.50 70-1301112.77
m+p Xylene mg/Kg wet0.10 5.00 70-1301145.69
o-Xylene mg/Kg wet0.050 2.50 70-1301132.83
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)11144.5
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)11646.2
[TOC_1]QC Data[TOC]
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B333760 - MA VPH
LCS Dup (B333760-BSD1) Prepared & Analyzed: 03/09/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10 7.50 2570-130124 4.049.27
Unadjusted C9-C12 Aliphatics mg/Kg wet10 7.50 2570-130113 3.138.48
C9-C10 Aromatics mg/Kg wet10 2.50 2570-130119 6.232.96
Benzene mg/Kg wet0.050 2.50 2570-130128 8.573.20
Butylcyclohexane mg/Kg wet0.050 2.50 2570-130119 2.162.98
Decane mg/Kg wet0.050 2.50 2570-13098.0 4.322.45
Ethylbenzene mg/Kg wet0.050 2.50 2570-130122 6.443.05
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050 2.50 2570-130120 7.882.99
2-Methylpentane mg/Kg wet0.050 2.50 25 L-0770-130134 6.86*3.36
Naphthalene mg/Kg wet0.50 2.50 2570-13093.8 12.22.35
Nonane mg/Kg wet0.050 2.50 2530-130122 3.153.05
Pentane mg/Kg wet0.050 2.50 2570-130114 4.702.85
Toluene mg/Kg wet0.050 2.50 2570-130124 7.543.09
1,2,4-Trimethylbenzene mg/Kg wet0.050 2.50 2570-130119 6.232.96
2,2,4-Trimethylpentane mg/Kg wet0.050 2.50 2570-130122 9.663.06
m+p Xylene mg/Kg wet0.10 5.00 2570-130121 5.916.03
o-Xylene mg/Kg wet0.050 2.50 2570-130120 6.013.01
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)12449.4
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)12851.0
Batch B333896 - MA VPH
[TOC_3]B333896[TOC]
Blank (B333896-BLK1) Prepared & Analyzed: 03/10/23
Unadjusted C5-C8 Aliphatics g/L100ND
C5-C8 Aliphatics g/L100ND
Unadjusted C9-C12 Aliphatics g/L100ND
C9-C12 Aliphatics g/L100ND
C9-C10 Aromatics g/L100ND
Benzene g/L1.0ND
Butylcyclohexane g/L1.0ND
Decane g/L1.0ND
Ethylbenzene g/L1.0ND
Methyl tert-Butyl Ether (MTBE)g/L1.0ND
2-Methylpentane g/L1.0ND
Naphthalene g/L5.0ND
Nonane g/L1.0ND
Pentane g/L1.0ND
Toluene g/L1.0ND
1,2,4-Trimethylbenzene g/L1.0ND
2,2,4-Trimethylpentane g/L1.0ND
m+p Xylene g/L2.0ND
o-Xylene g/L1.0ND
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)10140.6
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)10241.0
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B333896 - MA VPH
LCS (B333896-BS1) Prepared & Analyzed: 03/10/23
Unadjusted C5-C8 Aliphatics g/L100 150 70-130105157
Unadjusted C9-C12 Aliphatics g/L100 150 70-130100150
C9-C10 Aromatics g/L100 50.0 70-13010653.2
Benzene g/L1.0 50.0 70-13011155.4
Butylcyclohexane g/L1.0 50.0 70-13010954.4
Decane g/L1.0 50.0 70-13083.241.6
Ethylbenzene g/L1.0 50.0 70-13010954.5
Methyl tert-Butyl Ether (MTBE)g/L1.0 50.0 70-13011255.9
2-Methylpentane g/L1.0 50.0 70-13010954.6
Naphthalene g/L5.0 50.0 70-13094.147.0
Nonane g/L1.0 50.0 70-13010854.2
Pentane g/L1.0 50.0 70-13010954.7
Toluene g/L1.0 50.0 70-13010954.4
1,2,4-Trimethylbenzene g/L1.0 50.0 70-13010653.2
2,2,4-Trimethylpentane g/L1.0 50.0 70-13095.547.8
m+p Xylene g/L2.0 100 70-130109109
o-Xylene g/L1.0 50.0 70-13011155.3
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)11847.3
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)11747.0
LCS Dup (B333896-BSD1) Prepared & Analyzed: 03/10/23
Unadjusted C5-C8 Aliphatics g/L100 150 2570-130110 5.20166
Unadjusted C9-C12 Aliphatics g/L100 150 2570-130102 2.31154
C9-C10 Aromatics g/L100 50.0 2570-130112 4.7855.8
Benzene g/L1.0 50.0 2570-130114 3.1157.1
Butylcyclohexane g/L1.0 50.0 2570-130111 2.1855.6
Decane g/L1.0 50.0 2570-13084.8 1.9842.4
Ethylbenzene g/L1.0 50.0 2570-130114 4.5757.1
Methyl tert-Butyl Ether (MTBE)g/L1.0 50.0 2570-130114 2.0957.0
2-Methylpentane g/L1.0 50.0 2570-130115 5.0157.5
Naphthalene g/L5.0 50.0 2570-13095.7 1.7547.9
Nonane g/L1.0 50.0 2570-130111 2.7055.7
Pentane g/L1.0 50.0 2570-130116 6.0758.2
Toluene g/L1.0 50.0 2570-130113 3.6756.4
1,2,4-Trimethylbenzene g/L1.0 50.0 2570-130112 4.7855.8
2,2,4-Trimethylpentane g/L1.0 50.0 2570-13099.8 4.4149.9
m+p Xylene g/L2.0 100 2570-130114 4.41114
o-Xylene g/L1.0 50.0 2570-130116 4.3857.8
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)12249.0
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)12248.6
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FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Elevated reporting limit due to high concentration of target compounds. MA CAM reporting limit not met.RL-05
Surrogate recovery outside of control limits due to suspected sample matrix interference. Chromatogram(s) is
attached.
S-15
[TOC_1]Flag/Qualifier Summary[TOC]
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-VPH-Feb 2018 Rev 2.1 in Soil
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
MADEP-VPH-Feb 2018 Rev 2.1 in Water
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
[TOC_1]Certifications[TOC]
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
PH-0821Connecticut Department of Public HealthCT 12/31/2024
652North Carolina Div. of Water QualityNC 12/31/2023
MA00100State of MaineME 06/9/2023
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2023
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