MO-9144_40626_CA_MRP_20230330

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

March 30, 2023

Mr. Brad Newton
NCDEQ-UST Section
Mooresville Regional Office
610 East Center Ave.
Mooresville, NC 28115

Re: Ground Water Monitoring Report
January-February 2023
Kingsway #10
1418 West Garrison Boulevard
Gastonia, Gaston County
North Carolina
Facility ID Number: 0-00-0000003687
Incident Number: 40626
GRI Project Number: 4187

Dear Mr. Newton,

Please find enclosed the referenced report for the above-mentioned site.
If you have any questions, please contact Joanna Alley at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc. Mr. Mark King; Kingsway Enterprises, Inc., file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Ground Water Monitoring Report
January – February 2023
Kingsway #10
1418 West Garrison Boulevard
Gastonia, Gaston County
North Carolina
Facility ID Number: 0-00-0000003687
Incident Number: 40626
GRI Project Number: 4187

Prepared for:

Mr. Mark King
Kingsway Enterprises, Inc.
407 South Marietta Street
Gastonia, North Carolina 28052-4331

March 30, 2023

Joanna Alley, P.E.
Project Manager
Eric M. Eubanks, P.G.
Report Writer

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: March 30, 2023 Kingsway #10
Project Manager: Joanna Alley, P.E. GRI Project No. 4187
i
EXECUTIVE SUMMARY
Kingsway #10 is located at 1418 West Garrison Boulevard in Gastonia, Gaston County, North Carolina. The
site is currently owned and operated by Kingsway Enterprises, Inc. as a petroleum retail facility and
convenience store. A site check was conducted in May 2016 following a failed spill bucket that confirmed
the presence of a release. Currently, one 10,000-gallon gasoline, one 8,000-gallon gasoline, and one
6,000-gallon gasoline USTs are active at the site. The adjoining properties are residential and commercial.
According to the information determined during receptor survey activities, no water supply wells were
identified within 1,500 feet of the site. One unnamed ditch/creek feature is located approximately 390
feet northeast of the source area. Public water is available to the site and surrounding properties within
a 1,500-foot radius of the site.

The CAP has not been established for this site. Therefore, no cleanup milestones have been established.
A Feasibility Study was completed for the site in November 2019. Based on the study and subsequent free
product recovery events, MMPE is the current method of remediation.

Two simultaneous MMPE events were conducted at the site from January 9 to January 13, 2023, on
monitoring well MW-2 and recovery wells RW-1, RW-2, and RW-3. A total of 9,495 gallons of affected
ground water was recovered during the MMPE events. No measurable liquid phase free product was
recovered during either MMPE event. At the conclusion of the events, no free product was measured in
any of the vacuum wells or observation wells. The average fluid recovery rate was 98.91 gallons per hour.
Based on mass-removal calculations an additional 125.74 pounds or 20.97 gallons of vapor phase
hydrocarbons were removed at an average rate of 0.22 gallons per hour from the two MMPE systems.
Pre-MMPE ground water samples were collected from RW-1 through RW-3 on January 9, 2023. The
concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE, naphthalene, and/or 1,2-DCA reported
in the ground water samples collected from RW-1 through RW-3 exceeded the MACs. All contaminant
concentrations were below the GCLs. Free product measuring 0.03 feet thick was observed in MW-2.

On February 23, 2023, nineteen Type II monitoring wells, one Type III telescoping well, and three recovery
wells were gauged, purged, and/or sampled. Free product developed in monitoring wells MW-1 and MW-
2 during purging activities; therefore, these wells were not sampled. The concentrations of benzene,
toluene, ethylbenzene, xylenes, MTBE, naphthalene, TAA, bromodichloromethane, TBA,
dibromochloromethane, chloroform, EDB, 1,2-DCA, 1,2-dichloropropane, ethanol, isopropylbenzene, IPE,
n-propylbenzene, styrene, 1,1,2,2-tetrachloroethane, 1,2,4-trimethylbenzene, and/or 1,3,5-
trimethylbenzene reported in the ground water samples collected from MW-4, MW-5, MW-7, MW-9
through MW-11, MW-15, RW-1 through RW-3, and TW-1 exceeded the MACs. The concentrations of
benzene and/or EDB reported in the ground water samples collected from MW-9, MW-15, and RW-1
exceeded the GCLs. Although the reported concentrations of bromodichloromethane,
dibromochloromethane, and 1,1,2,2-tetrachloroethane exceeded the MACs, these compounds are not
considered to be petroleum constituents.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: March 30, 2023 Kingsway #10
Project Manager: Joanna Alley, P.E. GRI Project No. 4187
ii
Based on this information, the risk classification for the site should remain intermediate risk. MMPE
events should continue to be conducted at the site until free product is no longer present and contaminant
concentrations are below the GCLs. Semi-annual ground water monitoring should continue at the site.
The next sampling event is tentatively scheduled for August 2023.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: March 30, 2023 Kingsway #10
Project Manager: Joanna Alley, P.E. GRI Project No. 4187
iii
SITE INFORMATION
1. Site Identification
 Kingsway #10 (Facility ID 0-00-0000003687)
 Incident Number 40626 – Intermediate Risk (I130D)
 Location of Source Area: 1418 West Garrison Boulevard
Gastonia, NC 28052
Gaston County
35.257908°N, 81.207086°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST/AST Owner
Kingsway Enterprises, Inc.
407 South Marietta Street
Gastonia, NC 28052-4331
[e-mail]
704-864-7417

UST/AST Operator
Kingsway Enterprises, Inc.
407 South Marietta Street
Gastonia, NC 28052-4331
[e-mail]
704-864-7417

Property Owner
Kingsway Enterprises, Inc.
407 South Marietta Street
Gastonia, NC 28052-4331
[e-mail]
704-864-7417

Property Occupant
Kingsway Enterprises, Inc.
407 South Marietta Street
Gastonia, NC 28052-4331
[e-mail]
704-864-7417

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
Waypoint Analytical, LLC
449 Springbrook Road
Charlotte, NC 28217
State Cert. Nos. 37735 and 402
[phone]
3. Information about Release
 Release was discovered on August 22, 2016
 An unknown amount of product was released from the leaking UST System
 One 10,000-gallon gasoline, one 8,000-gallon gasoline, one 6,000-gallon gasoline USTs and
associated pumps and product piping are active at the site

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: March 30, 2023 Kingsway #10
Project Manager: Joanna Alley, P.E. GRI Project No. 4187
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: March 30, 2023 Kingsway #10
Project Manager: Joanna Alley, P.E. GRI Project No. 4187
TABLE OF CONTENTS
EXECUTIVE SUMMARY ....................................................................................................................... i
SITE INFORMATION ........................................................................................................................... iii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................2
3.0 FREE PRODUCT REMOVAL ........................................................................................................6
4.0 MMPE EVENT ..........................................................................................................................6
5.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................7
6.0 CONCLUSIONS .........................................................................................................................7
7.0 LIMITATIONS ...........................................................................................................................8
8.0 STATEMENTS AND CERTIFICATION ...........................................................................................9

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3A: Site Vicinity Map
Figure 3B: Zoning Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map
Figure 6: Benzene Isoconcentration Map
Figure 7: EDB Isoconcentration Map
Figure 8: Cross Section A-A’
Figure 9: Cross Section B-B’
Figure 10: Estimated Contaminant Mass Area Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Receptor Information
Table 4: Adjacent Property Owner Information
Table 5: Well Construction and Gauging Information
Table 6: Summary of Ground Water Sample Analytical Results
Table 7: Free Product Recovery Results
Table 8: Free Product Recovery Event Information
Table 9: Free Product Recovery Cost Summary

APPENDICES
Appendix A: State Correspondence
Appendix B: Land Use Information

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: March 30, 2023 Kingsway #10
Project Manager: Joanna Alley, P.E. GRI Project No. 4187
Appendix C: Incident Report
Appendix D: Historical Soil Quality Information
Appendix E: Laboratory Analytical Reports
Appendix F: Contaminant Mass Calculations
Appendix G: MMPE Report and Disposal Manifests

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: March 30, 2023 Kingsway #10
Project Manager: Joanna Alley, P.E. GRI Project No. 4187
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the January 2023 MMPE event and the February 2023 ground water sampling
event at the Kingsway #10 site, located at 1418 West Garrison Boulevard in Gastonia, Gaston County,
North Carolina (Figure 1). These activities were conducted in accordance with GRI Proposal No. 22-576,
which was submitted to the NCDEQ on September 26, 2022, and was approved as Task Authorization No.
40626-15 on October 21, 2022. State correspondence is included as Appendix A.

The site is currently owned and operated by Kingsway Enterprises, Inc. as a petroleum retail facility and
convenience store. A site check was conducted in May 2016 following a failed spill bucket that confirmed
the presence of a release. Currently, one 10,000-gallon gasoline, one 8,000-gallon gasoline and one 6,000-
gallon gasoline USTs are active at the site. UST owner/operator information and UST system information
are included as Tables 1 and 2, respectively. The Registered Tank Report is shown below:

The site and surrounding area are a mixture of commercial and residential properties. A copy of the Land
Use table is included as Appendix B. The site contains two buildings (the store and a car wash) and is
primarily capped with concrete and asphalt. The overall topography at the site is relatively flat and the
property drops off about 15 feet to the northeast. Nineteen Type II monitoring wells (MW-1 through MW-
19), one Type III monitoring well (TW-1) and three recovery wells (RW-1 through RW-3) were installed at
the site during previous ground water assessment activities. A Site Map showing the locations of the
monitoring wells and the structures on-site is included as Figure 2.

On December 14, 2016, GRI personnel conducted a receptor survey at the site. No water supply wells
were identified within 1,500 feet of the site. An unnamed creek is located approximately 390’ northeast
of the site. Municipal water is available to the site and surrounding properties. Receptor information is

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: March 30, 2023 Kingsway #10
Project Manager: Joanna Alley, P.E. GRI Project No. 4187
2
provided in Table 3. Adjacent property owner information is presented in Table 4. A Site Vicinity Map
showing the adjacent properties and a Zoning Map showing the zoning information have been included
as Figures 3A and 3B, respectively.

No previous incidents have been reported at the site. One incident (Incident No. 47766) has been reported
on an adjacent property. Copies of the NCDEQ Incident Reports are included as Appendix C. A map
showing the locations of additional incidents in the vicinity of the site is shown below:

A CAP has not been completed for the site. To date, two 8-hour AFVR events and seven 96-hour MMPE
events have been conducted at the site. A total of approximately 31,190.73 gallons of contaminated
ground water and free product have been removed from the site. A total of 1,018.73 gallons of free
product have been removed to date.

Based on this information, the site risk ranking was classified as Intermediate. Free product recovery
events should continue to be conducted at the site.
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
Soil assessment was not conducted during the current scope of work. Historical soil quality information
and soil excavation information is included as Appendix D.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: March 30, 2023 Kingsway #10
Project Manager: Joanna Alley, P.E. GRI Project No. 4187
3
On February 23, 2023, nineteen Type II monitoring wells (MW-1 through MW-19), one Type III telescoping
well (TW-1), and three recovery wells (RW-1 through RW-3) were gauged, purged, and/or sampled. Free
product developed in monitoring wells MW-1 and MW-2 during purging activities; therefore, these wells
were not sampled. Depths to ground water in the Type II monitoring wells and the recovery wells ranged
from 8.83 feet to 27.37 feet below TOC. Ground water elevations in the Type II monitoring wells and the
recovery wells ranged from 68.04 feet to 73.57 feet relative to an approximate datum of 100.00 feet
assigned to MW-1. Ground water flow was generally to the northeast with a horizontal gradient of
approximately 0.02 feet per foot between monitoring wells MW-7 and MW-18. The vertical gradient
between paired wells MW-1 and TW-1 was approximately 0.005 feet per foot in the upward direction.
Well construction and gauging information is presented in Table 5. A Water Table Surface Map based on
the Type II monitoring wells is included as Figure 4. A summary of the current ground water gauging data
is shown below:

Well ID Date
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
Comments
MW-1 2/23/2023 20 - 40 40 100.00 27.11 --- 72.89 GWS Event
MW-2 2/23/2023 20 - 40 40 99.80 27.21 --- 72.59 GWS Event
MW-3 2/23/2023 20 - 40 40 100.11 27.21 --- 72.90 GWS Event
MW-4 2/23/2023 20 - 40 40 100.27 27.20 --- 73.07 GWS Event
MW-5 2/23/2023 20 - 40 40 99.43 26.75 --- 72.68 GWS Event
MW-6 2/23/2023 20 - 40 40 99.19 26.17 --- 73.02 GWS Event
MW-7 2/23/2023 20 - 40 40 100.11 27.01 --- 73.10 GWS Event
MW-8 2/23/2023 20 - 40 40 99.87 26.30 --- 73.57 GWS Event
MW-9 2/23/2023 20 - 40 40 99.54 27.01 --- 72.53 GWS Event
MW-10 2/23/2023 20 - 40 40 97.66 25.37 --- 72.29 GWS Event
MW-11 2/23/2023 20 - 40 40 96.15 25.08 --- 71.07 GWS Event
MW-12 2/23/2023 20 - 40 40 97.85 26.29 --- 71.56 GWS Event
MW-13 2/23/2023 20 - 40 40 97.62 24.74 --- 72.88 GWS Event
MW-14 2/23/2023 10 - 30 30 85.00 13.65 --- 71.35 GWS Event
MW-15 2/23/2023 10 - 35 35 90.60 18.82 --- 71.78 GWS Event
MW-16 2/23/2023 10 - 30 30 78.70 10.15 --- 68.55 GWS Event
MW-17 2/23/2023 5 - 25 25 82.21 10.87 --- 71.34 GWS Event
MW-18 2/23/2023 5 - 25 25 76.87 8.83 --- 68.04 GWS Event
MW-19 2/23/2023 10 - 30 30 86.31 14.70 --- 71.61 GWS Event
RW-1 2/23/2023 20 - 35 35 100.09 27.13 --- 72.96 GWS Event
RW-2 2/23/2023 20 - 35 35 99.77 27.37 --- 72.40 GWS Event
RW-3 2/23/2023 20 - 40 40 NM 26.09 --- NM GWS Event
TW-1 2/23/2023 60 - 65 65 99.97 26.91 --- 73.06 GWS Event

Ground water samples collected from the monitoring wells were submitted for laboratory analyses using
EPA Method 6200B. The concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE, naphthalene,
TAA, bromodichloromethane, TBA, dibromochloromethane, chloroform, EDB, 1,2-DCA, 1,2-
dichloropropane, ethanol, isopropylbenzene, IPE, n-propylbenzene, styrene, 1,1,2,2-tetrachloroethane,
1,2,4-trimethylbenzene, and/or 1,3,5-trimethylbenzene reported in the ground water samples collected
from MW-4, MW-5, MW-7, MW-9 through MW-11, MW-15, RW-1 through RW-3, and TW-1 exceeded the

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: March 30, 2023 Kingsway #10
Project Manager: Joanna Alley, P.E. GRI Project No. 4187
4
MACs. The concentrations of benzene and/or EDB reported in the ground water samples collected from
MW-9, MW-15, and RW-1 exceeded the GCLs. Although the reported concentrations of
bromodichloromethane, dibromochloromethane, and 1,1,2,2-tetrachloroethane exceed the MACs, these
compounds are not considered to be petroleum constituents. A summary of the analytical results for
ground water samples collected on February 23, 2023, is presented in Table 6. A Ground Water Quality
Map based on the February 2023 data is included as Figure 5. A complete report of laboratory analyses
of the ground water samples collected from the monitoring wells during the February 2023
comprehensive sampling event are included as Appendix C. A summary of the current ground water
analytical data is shown below:

Contaminant of Concern  Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene EDB Well
ID
MACs (μg/l) 1 600 600 500 20 6 0.02
GCLs (μg/l) 5,000 260,000 80,000 50,000 20,000 6,000 50
10 Times 2B Standards (µg/l) 510 110 1,300 6,700 15,000 120 1
MW-1 FP FP FP FP FP FP FP
MW-2 FP FP FP FP FP FP FP
MW-3 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.200*
MW-4 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.200*
MW-5 92.4 18.7 32.8 178 669 9.72 J <2.00*
MW-6 <0.180 <0.220 <0.170 <0.210 1.05 <0.470 <0.200*
MW-7 <0.180 <0.220 <0.170 <0.210 3.11 <0.470 <0.200*
MW-8 0.941 <0.220 0.697 11.7 19.2 <0.470 <0.200*
MW-9 5,230 9,000 1,230 5,530 158 427 101*
MW-10 95.1 22.1 19.7 212 207 9.45 <0.200*
MW-11 19.0 <0.220 0.648 8.80 <0.140 1.32 <0.200*
MW-12 0.658 <0.220 0.597 6.00 57.6 1.15 <0.200*
MW-13 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.200*
MW-14 <0.180 <0.220 <0.170 <0.210 1.62 <0.470 <0.200*
MW-15 7,610 8,480 985 4,720 1,280 422 <20.0*
MW-16 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.200*
MW-17 <0.180 2.21 <0.170 <0.210 <0.140 1.07 <0.200*
MW-18 <0.180 <0.220 <0.170 <0.210 <0.140 2.77 <0.200*
MW-19 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.200*
TW-1 1.85 <0.220 0.460 J 0.501 <0.140 1.24 <0.200*
RW-1 6,800 25,400 2,380 14,400 <14.0 929 <20.0*
RW-2 6.51 64.4 17.0 236 90.4 12.1 <0.200*
RW-3 1,030 3,110 564 2,740 91.8 211 16.5*
Note: *: EDB results from Method 6200B analysis

The baseline contaminant mass at the site was determined based on the total BTEX, MTBE and
naphthalene concentrations from the May 26, 2017, September 26, 2017, and November 30, 2017, limited
ground water sampling events as well as the maximum historical water column height observed in each
area. The contaminant plume was divided into six areas (Areas 1 through 6) based on the benzene
concentrations during the May 26, 2017, September 26, 2017, and November 30, 2017, limited ground
water sampling events. Please note that the contaminant mass cannot be calculated in wells containing

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: March 30, 2023 Kingsway #10
Project Manager: Joanna Alley, P.E. GRI Project No. 4187
5
FP; therefore, the total contaminant mass in Area 2 is based on the known concentrations during the June
2022 sampling event, and the total contaminant mass is Area 3 is based off the contaminant
concentrations of MW-9. The dissolved contaminant mass has been reduced by 12.7%, 48.3%, 34.3%,
90.5%, and 100% in Areas 1, 3, 4, 5, and 6, respectively. The dissolved contaminant mass could not be
calculated for Area 2 because free product was encountered in MW-1. The total dissolved contaminant
mass for the site has decreased by 33.16% since 2017. To track total dissolved contaminant mass changes
more accurately, the eight monitoring wells that were used to define the contaminant mass should be
sampled at least annually. Contaminant mass calculations are included as Appendix D. A map of the
contaminant mass areas is included as Figure 6. A chart depicting the overall contaminant mass trend is
shown below:

The site is in the Kings Mountain Belt of foliated to massive granitic rocks within the Piedmont
Physiographic Province of North Carolina. The surficial aquifer in the vicinity of site directly overlies
massive granitic rock. The water table has a seasonal high depth to water of approximately 9 feet to 27
feet BGS.

Please note that while MMPE events have continued, a CAP has not been implemented at the site.
0.00
2.00
4.00
6.00
8.00
10.00
12.00
14.00
16.00
18.00
20.00
0.00
20,000.00
40,000.00
60,000.00
80,000.00
100,000.00
120,000.00
140,000.00
Average Water Column Height (ft)Contaminant Mass (grams)Time
Total Contaminant Mass vs. Time
Kingsway #10 (Incident No. 40626)
Contaminant Mass (grams)Water Column Height (ft)Linear (Contaminant Mass (grams))

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: March 30, 2023 Kingsway #10
Project Manager: Joanna Alley, P.E. GRI Project No. 4187
6
3.0 FREE PRODUCT REMOVAL
Free product has historically been present in monitoring wells MW-1 and MW-2 and recovery wells RW-
1 and RW-2. 8-hour AFVR events were conducted at the site in November 2017 and May 2018 to remove
free product. 96-hour MMPE events were conducted at the site in March 2019, April 2020, October 2020,
May 2021, May 2022, and January 2023. The January 2023 MMPE event is discussed below. To date,
approximately 1,019.22 gallons of liquid and vaporized petroleum product has been recovered. Free
product measuring approximately 0.01’ thick developed in MW-1 and MW-2 during the February 2023
ground water sampling event.
4.0 MMPE EVENT
Two simultaneous MMPE events were conducted at the site by Advanced Environmental Services, Inc.
under the supervision of GRI beginning on January 9, 2023, and ending on January 13, 2023. Monitoring
well MW-2 and recovery wells RW-1, RW-2, and RW-3 were used as extraction wells during the January
2023 MMPE events. The MMPE equipment for each event included a liquid ring pump, a 5,000-gallon
capacity and a 6,000-gallon capacity tankers, flexible vacuum hoses, a 2-inch and a 6-inch diameter
discharge stacks, 1.5-inch diameter PVC stinger pipes and associated couplings and pipe fittings to
manifold two separate systems to two wells simultaneously. The MMPE systems were rated at 130 CFM
at 21 in. Hg and 280 CFM at 25” Hg. All extraction wells were gauged prior to the start of the events. Free
product with a thickness of 0.03 feet was observed in MW-2 prior to the start of the MMPE events.
Elevated concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE, naphthalene, and/or IPE
were reported in the ground water samples collected from RW-1, RW-2, and RW-3 on January 9, 2023.
The stinger pipes depths remained constant at approximately 28 feet BGS in MW-1 and RW-1 through
RW-3 during the event.

Monitoring well MW-2 and recovery wells RW-1 through RW-3 were each vacuumed continuously for the
96-hour events. During the events, measurements of relative humidity, temperature, vacuum, exhaust
velocity and off-gas concentrations were recorded at the discharge stack of each MMPE unit a minimum
of two times per 24-hour period. Vacuum at extraction wells MW-2 and RW-1 remained steady at 18.0 in.
Hg, and the vacuum at extraction wells RW-2 and RW-3 ranged from 10.0 to 11.0 in. Hg. System vacuum
at MW-2 and RW-1 remained steady at 23.0 in. Hg, and the system vacuum at RW-2 and RW-3 ranged
from 14.0 to 15.0 in. Hg. The effluent velocity at MW-2 and RW-1 remained steady at 1,100 feet per
minute, and the effluent velocity at RW-2 and RW-3 ranged from 3,600 to 3,800 feet per minute. The
system temperature at MW-2 and RW-1 ranged from 108 to 124°F, and the system temperature at RW-2
and RW-3 ranged from 102 to 120°F. The relative humidity at MW-2 and RW-1 ranged from 56.0 to 72.0
percent, and the relative humidity at RW-2 and RW-3 remained steady at 99.0%. The VOC off-gas
concentrations at MW-2 and RW-1 ranged from 1,900 ppm to 5,500 ppm, and the off-gas concentrations
at RW-2 and RW-3 ranged from 600 ppm to 1,400 ppm during the event. No free product was measured
in any of the wells associated with the MMPEs after the 96-hour period. A summary of the gauging data
obtained before startup and at the conclusion of the MMPE event is presented in Table 5. A copy of the
MMPE report and calculations is included as Appendix E. A summary of the gauging data for the January
2023 MMPE event is listed below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: March 30, 2023 Kingsway #10
Project Manager: Joanna Alley, P.E. GRI Project No. 4187
7
MMPE
System Well ID
Product Thickness
before Recovery
(feet)
Product Thickness
after Recovery
(feet)
Amount of Liquid
Recovered
(gallons)
Amount of Product
Recovered as Liquid
(gallons)
A MW-2 0.03 0.00 5,810 0.00 RW-1 0.00 0.00
B RW-2 0.00 0.00 3,685 0.00 RW-3 0.00 0.00

The results of the MMPE events indicate that a total of 9,495 gallons of liquids were removed during the
event. Of the total liquids extracted, no measurable free product was removed during the events. Based
on 96 hours of operation, the average liquid recovery rate was 98.91 gallons per hour. Based on mass-
removal calculations, an additional 112.39 pounds or 18.27 gallons of vapor phase hydrocarbons were
removed from System A (MW-2 and RW-1), and an additional 13.35 pounds or 2.7 gallons of vapor phase
hydrocarbons were removed from System B (RW-2 and RW-3). Based on 96 hours of operation, an
average of 0.19 gallons of vapor phase hydrocarbons were removed per hour by MMPE System A, and
0.03 gallons of vapor phase hydrocarbons were removed per hour by MMPE System B. A summary of free
product recovery data has been included as Table 7. Summaries of MMPE event information and cost
analysis are provided in Tables 8 and 9, respectively. At the conclusion of the MMPE events, all
wastewater was transported to a licensed facility for disposal. Copies of the disposal manifests are
included in Appendix E. A summary of the free product recovery data from the January 2023 events is
listed below:

MMPE
System Well ID
Average
Effluent
Velocity
(ft/min)
Average
Effluent
Temperature
(°F)
Average Effluent
Concentration
(ppm)
Amount of
Vaporized
Product
(gallons)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered
as Liquid
(gallons)
Total
Amount of
Product
Recovered
(gallons)
A MW-2 1,100 120.44 2,666.67 18.27 5,810 0.00 18.27 RW-1
B RW-2 3,644.44 116.78 833.33 2.7 3,685 0.00 2.7 RW-3
Totals to Date 1,019.26 30,172.04 0.04 1,019.26

Based on these calculations, the MMPE was successful at reducing dissolved-phase petroleum
contaminant concentrations at the site.
5.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
MMPE events are being conducted at the site as the primary method of corrective action. Due to the site
being in the active remediation phase, no natural attenuation monitoring plan is currently in place at the
site.
6.0 CONCLUSIONS
 Two simultaneous MMPE events were conducted at the site from January 9 to January 13, 2023
on MW-2, RW-1, RW-2, and RW-3.
 A total of 9,495 gallons of affected ground water were recovered during the MMPE events. At the
conclusion of the events, no free product was measured in any of the wells associated with the

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: March 30, 2023 Kingsway #10
Project Manager: Joanna Alley, P.E. GRI Project No. 4187
8
MMPE events. The average liquid recovery rate was 98.91 gallons per hour. An additional 20.97
gallons of vapor phase hydrocarbons were removed at an average rate of 0.22 gallons per hour.
 Pre-MMPE ground water samples were collected from RW-1 through RW-3 on January 9, 2023.
The concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE, naphthalene, and/or IPE
reported in the ground water samples collected from RW-1 through RW-3 exceeded the MACs.
All contaminant concentrations were below the GCLs. Free product measuring 0.03 feet thick was
observed in MW-2.
 On February 23, 2023, nineteen Type II monitoring wells, one Type III telescoping well, and three
recovery wells were gauged, purged, and/or sampled. Free product developed in monitoring wells
MW-1 and MW-2 during purging activities; therefore, these wells were not sampled. Ground
water flow was generally to the northeast with a horizontal gradient of approximately 0.02 feet
per foot. The vertical gradient between paired wells MW-1 and TW-1 was approximately 0.005
feet per foot in the upward direction.
 The reported concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE, naphthalene,
TAA, bromodichloromethane, TBA, dibromochloromethane, chloroform, EDB, 1,2-DCA, 1,2-
dichloropropane, ethanol, isopropylbenzene, IPE, n-propylbenzene, styrene, 1,1,2,2-
tetrachloroethane, 1,2,4-trimethylbenzene, and/or 1,3,5-trimethylbenzene exceeded the MACs
in the ground water samples collected from MW-4, MW-5, MW-7, MW-9 through MW-11, MW-
15, RW-1 through RW-3, and TW-1 exceeded the MACs. The concentrations of benzene and/or
EDB reported in the ground water samples collected from MW-9, MW-15, and RW-1 exceeded
the GCLs.
 The dissolved contaminant mass has been reduced by 12.7%, 48.3%, 34.3%, 90.5%, and 100% in
Areas 1, 3, 4, 5, and 6, respectively. The dissolved contaminant mass could not be calculated for
Area 2 because free product was encountered in MW-1. The total dissolved contaminant mass
for the site has decreased by 33.16% since 2017.
 Based on this information, the risk classification for the site should remain intermediate risk.
MMPE events should continue to be conducted at the site until free product is no longer present
and contaminant concentrations are below the GCLs. Semi-annual ground water monitoring
should continue at the site. The next sampling event is tentatively scheduled for August 2023.
7.0 LIMITATIONS
This report has been prepared for the exclusive use of Kingsway Enterprises, Inc. for specific application
to the referenced site in Gaston County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by the NCDEQ and with resources adequate only for that scope
of work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would

FIGURES
Copyright:© 2013 National Geographic Society, i-cubed
FIGURE 1SITE LOCATION MAPKINGSWAY #101418 WEST GARRISON BOULEVARDGASTONIA, GASTON COUNTY,NORTH CAROLINAINCIDENT NO. 40626GRI PROJECT NO. 4187
PREPARED BY:GEOLOGICAL RESOURCES, INC.JANUARY 3, 201702,000 4,0001,000 Feet
SCALE: 1 INCH = 2,000 FEET
MAP CENTER LOCATIONLATITUDE: 35.257908° NLONGITUDE: 81.207086° W
`
SITE LOCATION
³
SITE
W GARRISON BLVD
W F R AN K L I N BLV D
S WEBB STLINWOOD RDS DALTON STS VANCE STFLOYD LNS GRAY STS YATES STS LIBERTY STS RANSOM STW FIFTH AVE
W S E C O N D AV E
W SEVENTH AVE
W FOURTH AVE
S BOYD STO V E R M A N A V E
W A I R L IN E A V E
P A R K D A L E A V E S MILLON STS FIRESTONE STW SIXTH AVE
S WELDON STS EMERSON STDRAKE STW M C F A R L A N D A V E GASTON AVEGRANT STN GRAY STW THIRD AVE
W SIXTH B AVE
N
Y
A
T
E
S
S
T
SUMMER DR
SYKES STN WEBB STROBI
NSON STWESTWYNN CIR
K
AYLO
R CT
EASTWYNN CIR
PHILLIPS CT
W F O U R T H A V E
W FOURTH AVE
S DALTON STO V ER M AN AVE
W SECOND AVE
S YATES STW F IF T H A V E S BOYD STS GRAY STS YATES STS MILLON ST42
4242
4 2
424242424 2
4242 42
3545161182 3545164158
3545151847
3545069254
3545068162
3545059913
3545162204
35451631303545152982
³
FIGURE 3A: SITE VICINITY MAPKINGSWAY #101418 WEST GARRISON BOULEVARDGASTONIA, GASTON COUNTYNORTH CAROLINAINCIDENT NO. 40626GRI PROJECT NO. 4187
PREPARED BY:GEOLOGICAL RESOURCES, INC.JANUARY 3, 2016
0 300150Feet
1 inch = 300 feet
NOTE:BASED ON DATA OBTAINED FROM GASTON COUNTY, NCGIS WEBSITE.
1,500-FOOT RADIUS
1,000-FOOT RADIUS
500-FOOT RADIUS
250-FOOT RADIUS
LEGEND
Street Centerline
RailRoad
Creek or Stream
Ponds
Subject Property
Adjacent Properties
Gaston County Parcels
2
5
4
1
1 Receptor Code
3
SITE
W GARRISON BLVD
W F R AN K L I N BLV D
S WEBB STLINWOOD RDS DALTON STS VANCE STFLOYD LNS GRAY STS YATES STS LIBERTY STS RANSOM STW FIFTH AVE
W S E C O N D AV E
W SEVENTH AVE
W FOURTH AVE
S BOYD STO V E R M A N A V E
W A I R L IN E A V E
P A R K D A L E A V E S MILLON STS FIRESTONE STW SIXTH AVE
S WELDON STS EMERSON STDRAKE STW M C F A R L A N D A V E GASTON AVEGRANT STN GRAY STW THIRD AVE
W SIXTH B AVE
N
Y
A
T
E
S
S
T
SUMMER DR
SYKES STN WEBB STROBI
NSON STWESTWYNN CIR
K
AYLO
R CT
EASTWYNN CIR
PHILLIPS CT
W F O U R T H A V E
W FOURTH AVE
S DALTON STO V ER M AN AVE
W SECOND AVE
S YATES STW F IF T H A V E S BOYD STS GRAY STS YATES STS MILLON ST4242
4 2
42424242³
FIGURE 3B: ZONING MAPKINGSWAY #101418 WEST GARRISON BOULEVARDGASTONIA, GASTON COUNTYNORTH CAROLINAINCIDENT NO. 40626GRI PROJECT NO. 4187
PREPARED BY:GEOLOGICAL RESOURCES, INC.MARCH 30, 2023
0 300150Feet
1 inch = 300 feetNOTE:BASED ON DATA OBTAINED FROM GASTON COUNTY, NCGIS WEBSITE.
1,500-FOOT RADIUS
1,000-FOOT RADIUS
500-FOOT RADIUS
250-FOOT RADIUS
LEGEND
Street Centerline
RailRoad
Creek or Stream
Ponds
ZONING - C-3 CD
ZONING - RS-8
ZONING - UMU
ZONING -I-U
ZONING - I-1 CD
ZONING - RMF
ZONING - C-3
ZONING - C-1
ZONING - O-1
Gaston County Parcels2
5
4
1
1 Receptor Code
3

TABLES
UST ID Number 1 - 3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1 - 3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1 - 3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1 - 3 Facility ID Number
Owner or Operator?
Owner/Operator
TABLE 1
UST OWNER/OPERATOR INFORMATION
KINGSWAY #10 (INCIDENT NO. 40626)
407 South Marietta Street Gastonia, NC 28052-4331 [phone]
00-0-0000003687
Dates of Ownership / OperationName of Owner or Operator
Address Telephone Number
Kingsway Enterprises, Inc. 05/01/2000 to Present
00-0-0000003687
Name of Owner or Operator Dates of Ownership / Operation
O'Hair Donald C. Muriel 04/01/1990 to 5/1/2000
Address Telephone Number
NA NA
00-0-0000003687
Name of Owner or Operator Dates of Ownership / Operation
Waters Inc. 10/01/1989 to 04/01/1990
Address Telephone Number
NA NA
00-0-0000003687
Name of Owner or Operator Dates of Ownership / Operation
Roberts Enterprises 05/04/1977 to 10/01/1989
Address Telephone Number
NA NA
Page 1 of 1
Date: 05/29/18 00-0-0000003687
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline Gasoline 10,000 05/04/77 Steel 8' x 26.6"
Double Wall
Flex Current Unknown
2 Gasoline Gasoline 8,000 05/04/77 Steel 8' x 21.3"
Double Wall
Flex Current Yes
3 Gasoline Gasoline 6,000 05/04/77 Steel 8' x 16'
Double Wall
Flex Current Unknown
Notes:
Data obtained from the NCDEQ registered tank database.
KINGSWAY #10 (INCIDENT NO. 40626)
Facility ID # :
TABLE 2
UST SYSTEM INFORMATION
Capacity
(gallons)
Tank
Dimensions
Status
of
UST
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Construction
Details
Description of
Associated
Product Piping
and
Pumps
Date
Installed
Page 1 of 1
Facility ID # : 00-0-0000003687
Receptor
ID
Latitude/
Longitude of
Any
Significant
Points
Up or Down-
Gradient
Distance
from
the source
area
of release
(ft.)
1 n/a Down ~390 NE
Notes:
• Receptors are shown on Figure 3A.
• n/a: not applicable.
TABLE 3
RECEPTOR INFORMATION
KINGSWAY #10 (INCIDENT NO. 40626)
Date: 07/26/22
Unnamed creek Starts northeast of the site and flows to the east n/a Drainage
Description Location
Contact/Phon
e Number Usage
Page 1 of 1
Date: 07/26/22 Facility ID # : 00-0-0000003687
3545-16-1182 (site) Kingsway Enterprises, Inc.
407 South Marietta Street
Gastonia, NC 28052
3545-16-2204 Joel & Lisa Lipscomb
316 Linwood Road
Gastonia, NC 28052
3545-16-4158 PlannerX, LLC
1331 East Garrison Blvd, Suite C
Gastonia, NC 28052
3545-16-3130 PlannerX, LLC
1331 East Garrison Blvd, Suite C
Gastonia, NC 28052
3545-15-2982 Lawrence & Judith Johnson 1616 Burke Road
Shelby, NC 28152
3545-06-9253 Amelia J. Prescott
977 Robinson Road
Gastonia, NC 28056
3545-06-8162 Industrial Electroplating Co.
P.O. Box 1537
Gastonia, NC 28053-1537
3545-15-1847 Keith Hoogland LTD. Partnership
1022 East Adams Street
Springfield, IL 62703
3545-05-9913 Jay Umiya, LLC.
3562 Fieldstone Drive
Gastonia, NC 28056
Note:
• Properties are keyed to Figure 3A.
TABLE 4
ADJACENT PROPERTY OWNER INFORMATION
KINGSWAY #10 (INCIDENT NO. 40626)
Pin Number Property Owner Name Mailing Address
Date: 03/17/23
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water from
Top of
Casing
(ft)
Free Product
Thickness**
(ft.)
Ground
Water
Elevation
(ft.)
Comments
12/13/16 NM 29.32 ---NM Sheen
05/26/17 29.61 ---70.39
11/20/17 31.67 1.47 69.59 Pre-AFVR
11/20/17 31.57 ---68.43 Post-AFVR
11/30/17 30.84 0.33 69.44
05/02/18 30.89 0.90 69.88 Pre-AFVR
05/02/18 32.47 ---67.53 Post-AFVR
05/22/18 29.68 0.10 70.41
10/25/18 28.25 ---71.75
01/07/19 26.57 Sheen 73.43
03/25/19 24.90 ---75.10 Pre-MMPE
03/29/19 24.71 ---75.29 Post-MMPE
05/08/19 24.51 ---75.49
04/13/20 25.57 ---74.43 OBS Well
04/17/20 26.62 ---73.38 OBS Well
05/20/20 25.11 0.04 74.92
10/26/20 25.26 ---74.74 OBS Well
12/01/20 25.36 ---74.64
05/10/21 23.98 ---76.02 OBS Well
05/14/21 23.98 ---76.02 OBS Well
06/14/21 24.21 ---75.79
06/21/22 26.87 ---73.13
01/09/23 27.98 ---72.02 Pre-MMPE
01/13/23 29.05 ---70.95 Post-MMPE
02/23/23 27.11 ---72.89
05/26/17 29.66 0.02 70.16
09/26/17 30.37 0.19 69.59 Free Product Test
11/20/17 30.70 0.04 69.13 Pre-AFVR
11/20/17 31.98 ---67.82 Post-AFVR
11/30/17 30.71 0.01 69.10
05/02/18 29.81 Sheen 69.99 Pre-AFVR
05/02/18 30.39 ---69.41 Post-AFVR
05/22/18 29.61 Sheen 70.19
10/25/18 28.98 Sheen 70.82
01/07/19 27.13 Sheen 72.67
03/25/19 25.48 ---74.32 Pre-MMPE
03/29/19 25.58 ---74.22 Post-MMPE
05/08/19 25.26 Sheen 74.54
04/13/20 25.85 ---73.95 OBS Well
04/17/20 26.15 ---73.65 OBS Well
05/20/20 26.02 0.01 73.79
10/26/20 25.69 ---74.11 OBS Well
12/01/20 25.75 ---74.05
05/10/21 24.40 ---75.40 OBS Well
05/14/21 24.40 ---75.40 OBS Well
06/14/21 24.69 ---75.11
06/21/22 27.15 ---72.65
01/09/23 28.03 0.03 71.80 Pre-MMPE
01/13/23 31.54 ---68.26 Post-MMPE
02/23/23 27.21 ---72.59
05/26/17 29.83 ---70.28
11/20/17 30.59 ---69.52 OBS Well
11/20/17 30.84 ---69.27 OBS Well
11/30/17 30.64 ---69.47
05/02/18 30.01 ---70.10 OBS Well
05/02/18 30.04 ---70.07 OBS Well
05/22/19 29.79 ---70.32
03/25/19 25.32 ---74.79 OBS Well
03/29/19 25.39 ---74.72 OBS Well
04/13/20 26.00 ---74.11 OBS Well
04/17/20 26.18 ---73.93 OBS Well
06/14/21 24.84 ---75.27
01/09/23 28.04 ---72.07 Pre-MMPE
01/13/23 28.42 ---71.69 Post-MMPE
02/23/23 27.21 ---72.90
05/26/17 29.80 ---70.47
11/20/17 30.73 ---69.54 OBS Well
11/20/17 30.77 ---69.50 OBS Well
11/30/17 30.77 ---69.50
05/02/18 30.03 ---70.24 OBS Well
05/02/18 30.12 ---70.15 OBS Well
05/22/18 29.77 ---70.50
06/14/21 24.45 ---75.82
02/23/23 27.20 ---73.07
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
KINGSWAY #10 (INCIDENT NO. 40626)
Facility ID # : 00-0-0000003687
MW-1 12/13/16 20 20 - 40 40 100.00
99.80MW-2 05/25/17 20 20 - 40 40
MW-3 05/25/17
MW-4 05/25/17
20 20 - 40 40 100.11
20 20 - 40 40 100.27
Page 1 of 4
Date: 03/17/23
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water from
Top of
Casing
(ft)
Free Product
Thickness**
(ft.)
Ground
Water
Elevation
(ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
KINGSWAY #10 (INCIDENT NO. 40626)
Facility ID # : 00-0-0000003687
05/26/17 29.21 ---70.22
11/30/17 30.27 ---69.16
05/02/18 29.38 ---70.05 OBS Well
05/02/18 29.41 ---70.02 OBS Well
05/22/18 29.18 ---70.25
03/25/19 25.23 --- 74.20 OBS Well
03/29/19 25.25 ---74.18 OBS Well
04/13/20 25.31 ---74.12 OBS Well
04/17/20 25.42 ---74.01 OBS Well
06/14/21 23.91 ---75.52
06/21/22 26.62 ---72.81
02/23/23 26.75 ---72.68
05/26/17 28.76 ---70.43
11/30/17 29.81 ---69.38
05/22/18 28.75 ---70.44
04/13/20 24.73 ---74.46 OBS Well
04/17/20 24.81 ---74.38 OBS Well
06/14/21 23.18 ---76.01
06/21/22 26.08 ---73.11
02/23/23 26.17 ---73.02
05/26/17 29.54 ---70.57
11/20/17 30.53 ---69.58 OBS Well
11/20/17 30.53 ---69.58 OBS Well
11/30/17 30.57 ---69.54
05/22/18 29.51 ---70.60
03/25/19 25.06 ---75.05 OBS Well
03/29/19 25.09 ---75.02 OBS Well
04/13/20 25.43 ---74.68 OBS Well
04/17/20 25.58 ---74.53 OBS Well
06/14/21 24.86 ---75.25
06/21/22 26.76 ---73.35
02/23/23 27.01 ---73.10
09/26/17 29.27 ---70.60
11/30/17 29.83 ---70.04
05/22/18 28.73 ---71.14
06/14/21 24.49 ---75.38
06/21/22 26.20 ---73.67
02/23/23 26.30 ---73.57
09/26/17 30.08 ---69.46
11/20/17 30.53 ---69.01 Pre-AFVR
11/20/17 32.06 ---67.48 Post-AFVR
11/30/17 30.57 ---68.97
05/02/18 29.63 ---69.91 Pre-AFVR
05/02/18 31.86 ---67.68 Post-AFVR
05/22/18 29.42 ---70.12
10/25/18 28.88 ---70.66
01/07/19 26.97 ---72.57
03/25/19 25.31 ---74.23 Pre-MMPE
03/29/19 25.45 ---74.09 Post-MMPE
05/08/19 25.16 ---74.38
04/13/20 25.68 ---73.86 OBS Well
04/17/20 26.72 ---72.82 OBS Well
05/20/20 26.21 ---73.33
12/01/20 25.68 ---73.86
06/14/21 24.62 ---74.92
05/23/22 27.11 ---72.43
05/27/22 29.52 ---70.02
06/21/22 26.93 ---72.61
01/09/23 27.85 ---71.69 Pre-MMPE
01/13/23 30.24 ---69.30 Post-MMPE
02/23/23 27.01 ---72.53
09/26/17 28.86 ---68.80
11/30/17 29.17 ---68.49
05/22/18 27.80 ---69.86
10/25/18 27.63 ---70.03
01/07/19 25.46 ---72.20
05/08/19 24.00 ---73.66
05/20/20 25.13 ---72.53
12/01/20 24.26 ---73.40
06/14/21 23.24 ---74.42
06/21/22 25.58 ---72.08
02/23/23 25.37 ---72.29
MW-10 09/20/17
MW-5 05/25/17
MW-6 05/25/17
MW-7 05/25/17
MW-8 09/20/17
MW-9 09/20/17
20 - 40
20 20 - 40 40 99.43
20 20 - 40 40 99.19
20 20 - 40 40 100.11
20 40 99.87
20 20 - 40 40 99.54
20 20 - 40 40 97.66
Page 2 of 4
Date: 03/17/23
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water from
Top of
Casing
(ft)
Free Product
Thickness**
(ft.)
Ground
Water
Elevation
(ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
KINGSWAY #10 (INCIDENT NO. 40626)
Facility ID # : 00-0-0000003687
11/30/17 28.68 ---67.47
05/22/18 27.29 ---68.86
06/14/21 22.75 ---73.40
06/21/22 25.37 ---70.78
02/23/23 25.08 ---71.07
11/30/17 29.95 ---67.90
05/22/18 28.69 ---69.16
06/14/21 24.24 ---73.61
06/21/22 26.45 ---71.40
02/23/23 26.29 ---71.56
11/30/17 28.53 ---69.09
05/22/18 27.39 ---70.23
06/14/21 22.86 ---74.76
02/23/23 24.74 ---72.88
11/30/17 17.29 ---67.71
05/22/18 15.98 ---69.02
10/25/18 15.76 ---69.24
01/07/19 13.78 ---71.22
05/08/19 12.55 ---72.45
05/20/20 13.27 ---71.73
12/01/20 12.71 ---72.29
06/14/21 11.83 ---73.17
06/21/22 13.75 ---71.25
02/23/23 13.65 ---71.35
11/30/17 22.23 ---68.37
05/22/18 21.07 ---69.53
10/25/18 20.76 ---69.84
01/07/19 18.91 ---71.69
05/08/19 17.54 ---73.06
05/20/20 17.93 ---72.67
12/01/20 17.17 ---73.43
06/14/21 16.91 ---73.69
06/21/22 19.62 ---70.98
02/23/23 18.82 ---71.78
05/22/18 11.64 ---67.06
06/14/21 9.37 ---69.33
02/23/23 10.15 ---68.55
05/22/18 13.11 ---69.10
06/14/21 9.67 ---72.54
02/23/23 10.87 ---71.34
05/22/18 10.66 ---66.21
06/14/21 7.85 ---69.02
02/23/23 8.83 ---68.04
05/22/18 17.08 ---69.23
10/25/18 16.81 ---69.50
01/07/19 14.98 ---71.33
05/08/19 13.91 ---72.40
05/20/20 14.04 ---72.27
12/01/20 13.25 ---73.06
06/14/21 13.27 ---73.04
02/23/23 14.70 ---71.61
90.60
MW-11 11/06/17
MW-12 11/06/17
10 10 - 35 35
MW-13 11/29/17
MW-14 11/29/17
MW-15 11/29/17
MW-16 05/21/18
MW-17 05/21/18
MW-18 05/21/18
MW-19 05/21/18
20 20 - 40 40 96.15
20 20 - 40 40 97.85
20 20 - 40 40 97.62
10 10 - 30 30 85.00
10 10 - 30 30 78.70
5 5 - 25 25 82.21
5 5 - 25 25 76.87
10 10 - 30 30 86.31
Page 3 of 4
Date: 03/17/23
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water from
Top of
Casing
(ft)
Free Product
Thickness**
(ft.)
Ground
Water
Elevation
(ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
KINGSWAY #10 (INCIDENT NO. 40626)
Facility ID # : 00-0-0000003687
05/26/17 29.44 ---70.53
11/30/17 30.45 ---69.52
05/22/18 31.64 ---68.33
06/14/21 24.49 ---75.48
06/21/22 26.93 ---73.04
02/23/23 26.91 ---73.06
04/13/20 25.59 ---74.50 Pre-MMPE
04/17/20 26.20 ---73.89 Post-MMPE
05/20/20 25.34 0.05 74.79
10/26/20 25.09 ---75.00 Pre-MMPE
10/30/20 28.76 ---71.33 Post-MMPE
12/01/20 25.33 ---74.76
05/10/21 23.94 ---76.15 Pre-MMPE
05/14/21 27.41 ---72.68 Post-MMPE
06/14/21 24.19 ---75.90
06/21/22 26.90 ---73.19
01/09/23 27.90 ---72.19 Pre-MMPE
01/13/23 30.24 ---69.85 Post-MMPE
02/23/23 27.13 ---72.96
04/13/20 25.96 ---73.81 Pre-MMPE
04/17/20 26.11 ---73.66 Post-MMPE
05/20/20 25.47 0.02 74.32
10/26/20 25.79 ---73.98 Pre-MMPE
10/30/20 28.81 ---70.96 Post-MMPE
12/01/20 25.99 ---73.78
05/10/21 24.40 ---75.37 Pre-MMPE
05/14/21 27.53 ---72.24 Post-MMPE
06/14/21 24.87 ---74.90
06/21/22 27.27 ---72.50
01/09/23 28.17 ---71.60 Pre-MMPE
01/13/23 30.28 ---69.49 Post-MMPE
02/23/23 27.37 ---72.40
05/23/22 27.04 ---NM
05/27/22 27.78 ---NM
06/21/22 26.95 ---NM
01/09/23 27.72 ---NM Pre-MMPE
01/13/23 30.80 ---NM Post-MMPE
02/23/23 26.09 ---NM
Notes:
• ft BGS : feet below ground surface.
• NM: Not Measured.
• *: Reference point for elevation measurements, assumed elevation 100.00 ft.
• ** : If free product is present in a well, ground water elevation calculated by: [Top of Casing Elevation - Depth to Water] + [free
RW-3 11/20/21
20 20 - 35 35 99.77
20 20 - 40 40 NM
TW-1 05/25/17
RW-1 03/31/20
RW-2 03/31/20
20 20 - 35 35 100.09
60 60 - 65 65 99.97
Page 4 of 4
Date: 3/17/23
EPA
504.1
SW846
6010B
Well ID
Date
Collected(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 4 10 70 70 0.4 70 3 6 0.4 0.6 4,000 70 70 25 70 70 0.005 400 400 0.02 15 400 400 700 700 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 ######NE 4,000 10,000 5,900 8,800 400 70,000 3,000 405 400 600 4,000,000 30,500 70,000 11,700 26,100 70,000 NE 28,500 24,100 50 15,000 NE NE NE NE NE
510 110 1,300 6,700 15,000 120 NE NE 270 1,200 NE 39 NE 210 20,000 110,000 1,000 6,500 310 50,000 2,500 NE NE 800 NE 0.01 3,900 2,150 1 5.4 1,250 NE 1,800 NE 40,00012/13/16 8,910 18,900 2,260 11,700 49.7 758 NR NR ****NR 16.9 J 9.1 J ********72.7 **NR 76.1 323 **230 184 **1,620 402 176 403 47,300 7350 J 7,350 J 11,300 05/26/17 22,800 37,400 3,810 18,400 1,120 1,030 NR NR ****NR 61.8 J <31 ********599 **NR 132 2,060 **433 184 **3,330 816 930*NR NR NR NR NR NR05/02/18 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP **FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP05/22/18 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP **FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP10/25/18 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS **NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS01/07/19 11,900 21,700 2,700 11,500 289 1,150 1,920 <20 ****<200 53.4 20.4 J ********147 **<6,500 108 542 **360 149 **2,890 689 269*NR NR NR NR NR NR03/25/19 14,800 31,800 3,030 15,000 1,400 556 8,260 J <200 ****<2,000 <130 <130 ********428 J **<65,000 <130 1,070 **288 J <130 **1,830 564 592*NR NR NR NR NR NR05/08/19 19,700 33,500 3,600 17,900 1,040 954 6,850 <100 ****<1,000 <63 <63 ********362 **<33,000 125 J 1,250 **368 <63 **2,920 781 367*NR NR NR NR NR NR05/20/20 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
12/01/20 9,980 27,200 2,840 15,300 <63 968 2,580 J <100 ****<1,000 <63 <63 ********127 J **<33,000 75.8 J 290 **255 105 J <63 2,220 611 383*NR NR NR NR NR NR06/14/21 8,260 53,700 25,400 172,000 <130 65,800 <2,000 <130 <130 <2,000 3,640 1,220 <130 <130 **<130 <130 <130 <65,000 2,190 207 J 536 13,000 241 J <130 154,000 31,300 <130*NR NR NR NR NR NR
06/21/22 13,200 E 39,200 E 2,810 13,600 427 1,050 3,510 <20 <13 <13 <200 49.1 J 22.1 J <13 <13 56.0 <13 117 <13 <6500 109 478 <13 346 141 <13 2,750 704 446*NR NR NR NR NR NR02/23/23 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/26/17 FP FP FP FP FP FP FP FP ****FP FP FP ********FP **FP FP FP **FP FP **FP FP FP FP FP FP FP FP FP05/02/18 7,480 15,500 2,170 12,700 770 818 NR NR ****NR <63 <63 ********105 J **NR 85.2 J 420 **251 106 J **2,330 606 198 J*NR NR NR NR NR NR
05/22/18 2,850 6,020 1,280 7,610 380 788 NR NR ****NR 48.8 J 18.9 J ********60.8 **NR 76.7 215 **229 56.6 **2,170 588 95.4*NR NR NR NR NR NR10/25/18 9,590 15,700 2,130 11,200 1,870 769 3,280 55.7 J ****<500 65.0 J <31 ********150 **53,800 97.1 J 524 **325 95.9 J **2,510 621 410*NR NR NR NR NR NR
01/07/19 2,120 3,610 938 4,800 441 388 693 J <20 ****<200 43.6 J 16.6 J ********50.7 **9,240 J 68.8 166 **215 <13 **1,710 470 <13* NR NR NR NR NR NR03/25/19 2,740 3,960 1,010 5,350 536 464 917 J <20 ****<200 45.0 J 18.4 J ********57.6 **10,300 64.3 211 **250 <13 **1,870 485 71.0*NR NR NR NR NR NR05/08/19 9,840 12,000 1,390 6,910 1,760 493 3,110 63.8 J ****<200 <13 13.7 J ********135 **20,600 68.1 567 **215 <13 **1,650 423 236*NR NR NR NR NR NR05/20/20 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP **FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
12/01/20 3,140 5,650 1,140 6,000 362 555 <200 <20 ****<200 48.6 J 19.8 J ********33.2 J **<6,500 61.6 130 **254 37.6 J **2,020 550 64.3*NR NR NR NR NR NR06/14/21 3,470 6,280 1,050 5,680 353 416 <400 <25 <25 <400 37.9 J <25 <25 <25 **<25 36.4 J <25 <13,000 41.9 J 114 <25 201 <25 <25 1,550 381 65.8 J*NR NR NR NR NR NR
06/21/22 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP02/23/23 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP05/26/17 8.0 45.1 18.9 96.5 0.68 12.3 NR NR ****NR 2.1 0.69 ********<0.13 **NR 1.9 1.6 **7.8 <0.13 **46.6 15.0 0.36 183 NR NR NR NR NR06/14/21 <0.13 <0.13 <0.13 <0.25 0.57 <0.13 <2.0 NM <0.13 <0.13 <2.0 <0.13 <0.13 <0.13 0.31 J **<0.13 <0.13 <0.13 <65 <0.13 0.33 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13*NR NR NR NR NR NR02/23/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.50 <1.60 <0.180 <0.200 <0.190 2.36 <0.220 <0.210 <0.150 <0.190 <42.0 <0.180 <0.500 <0.089 <0.190 <0.220 <0.270 <0.190 <0.180 <0.200*NR NR NR NR NR NR05/26/17 2.5 8.6 2.6 13.4 0.43 J 1.9 NR NR ****NR 0.25 J <0.13 ********<0.13 **NR 0.19 J 0.70 **0.82 <0.13 **7.5 2.0 0.25 28.1 NR NR NR NR NR06/14/21 0.20 J <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 NM 2.7 <0.13 <2.0 <0.13 <0.13 0.26 J 16.2 **<0.13 <0.13 <0.13 <65 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13*NR NR NR NR NR NR02/23/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 4.75 <1.50 <1.60 <0.180 <0.200 <0.190 30.1 <0.220 <0.210 <0.150 <0.190 <42.0 <0.180 <0.500 <0.089 <0.190 <0.220 <0.270 <0.190 <0.180 <0.200*NR NR NR NR NR NR05/26/17 341 120 61.3 496 506 15.1 NR NR ****NR 1.2 J 0.91 J ********48.2 **NR 6.4 222 **8.4 <0.63 **120 18.9 2.3 66.0 NR NR NR NR NR06/14/21 183 141 80.5 397 1,050 6.4 J 1,750 NR 15.7 14.4 <50 <3.1 <3.1 13.6 167 **16.6 28.5 7.2 J <1,600 3.6 J 159 <3.1 10.0 J <3.1 <3.1 58.9 25.8 <3.1*NR NR NR NR NR NR06/21/22 1,760 656 802 3,750 10,600 119 J 11,000 156 J 154 145 <500 <31 <31 125 J 1,760 89.8 J 185 276 72.5 J <16000 47.4 J 1,520 <31 109 J <31 <31 1140 278 <31*NR NR NR NR NR NR02/23/23 92.4 18.7 32.8 178 669 9.72 J 1,580 19.6 J 11.2 <15.0 822 <1.80 <2.00 <1.90 119 <2.20 <2.10 19.6 <1.90 <420 3.43 J 139 <0.890 5.03 <2.20 <2.70 44.3 21.1 <2.00*NR NR NR NR NR NR05/26/17 0.40 J 0.58 0.30 J 1.9 1.3 0.27 J NR NR ****NR <0.13 <0.13 ********0.27 J **NR <0.13 9.9 **<0.13 <0.13 **0.63 0.44 J 0.46 29.9 NR NR NR NR NR06/14/21 <0.13 <0.13 <0.13 <0.25 1.4 <0.13 76.7 NR <0.13 <0.13 27.6 <0.13 <0.13 <0.13 0.35 J **<0.13 0.14 J <0.13 <65 <0.13 3.3 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13*NR NR NR NR NR NR06/21/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 <0.13 <2.0 <0.13 <0.13 <0.13 <0.13 <0.20 <0.13 <0.13 <0.13 <65 <0.13 0.79 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13* NR NR NR NR NR NR02/23/23 <0.180 <0.220 <0.170 <0.210 1.05 <0.470 <1.90 <0.280 <0.160 <1.50 <1.60 <0.180 <0.200 <0.190 <0.220 <0.220 <0.210 <0.150 <0.190 <42.0 <0.180 1.14 <0.089 <0.190 <0.220 <0.270 <0.190 <0.180 <0.200*NR NR NR NR NR NR05/26/17 2.5 3.7 4.4 12.6 3.2 0.89 NR NR ****NR 0.18 J <0.13 ********3.1 **NR 0.57 38.2 **1.2 <0.13 **2.2 2.3 0.50 203 NR NR NR NR NR06/14/21 <0.13 <0.13 <0.13 <0.25 4.9 <0.13 28.5 NR <0.13 <0.13 29.8 <0.13 <0.13 <0.13 0.40 J **<0.13 1.6 <0.13 <65 <0.13 13.2 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13*NR NR NR NR NR NR06/21/22 <0.13 <0.13 <0.13 <0.25 1.9 <0.13 3.7 J <0.20 <0.13 <0.13 22.7 <0.13 <0.13 <0.13 0.29 J <0.20 <0.13 0.45 J <0.13 <65 <0.13 6.1 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR02/23/23 <0.180 <0.220 <0.170 <0.210 3.11 <0.470 <1.90 <0.280 <0.160 <1.50 44.9 <0.180 <0.200 <0.190 <0.220 <0.220 <0.210 <0.150 <0.190 <42.0 <0.180 6.85 <0.089 <0.190 <0.220 <0.270 <0.190 <0.180 <0.200*NR NR NR NR NR NR09/26/17 66.1 4.4 21.6 398 249 42.2 NR NR ****NR 0.90 0.59 ********1.4 **NR 3.3 11.7 **7.8 <0.13 **117 29.6 0.11 36.5 NR NR NR NR NR06/14/21 3.6 0.25 J 1.1 28.6 10.9 0.68 2.0 J NR <0.13 <0.13 <2.0 <0.13 <0.13 <0.13 1.2 **<0.13 0.20 J <0.13 <65 0.20 J 2.4 <0.13 0.35 J <0.13 <0.13 5.1 1.9 <0.13*NR NR NR NR NR NR06/21/22 2.5 <0.13 0.72 21.0 12.7 0.59 <2.0 0.49 J <0.13 <0.13 <2.0 <0.13 <0.13 <0.13 1.5 <0.20 <0.13 0.23 J <0.13 <65 0.16 J 3.3 <0.13 0.18 J <0.13 <0.13 6.2 2.5 <0.13* NR NR NR NR NR NR02/23/23 0.941 <0.220 0.697 11.7 19.2 <0.470 <1.90 1.68 J <0.160 <1.50 <1.60 <0.180 <0.200 <0.190 2.46 <0.220 <0.210 <0.150 <0.190 <42.0 <0.180 4.66 <0.089 <0.190 <0.220 <0.270 2.58 2.92 <0.200*NR NR NR NR NR NR09/26/17 8,890 20,800 3,570 17,800 2,450 1,470 NR NR ****NR 41.8 J <25 ********157 **NR 132 578 **385 187 **3,210 805 70.4 548 NR NR NR NR NR05/02/18 7,970 15,900 2,020 9,910 2,520 580 NR NR ****NR <63 <63 ********145 J **NR <63 516 **208 J 115 J **1,460 399 153 J*NR NR NR NR NR NR05/22/18 6,610 11,300 1,340 7,500 1,610 514 NR NR ****NR <25 <25 ********107 **NR 56.8 J 407 **154 89.5 J **1,310 343 152*NR NR NR NR NR NR10/25/18 7,170 12,500 1,430 7,190 1,690 472 2,880 100 J ****<500 <31 <31 ********126 J **<16,000 46.4 J 417 **140 83.8 J **1,140 272 148*NR NR NR NR NR NR01/07/19 14,000 19,500 1,950 9,350 1,610 635 3,620 J <100 ****<1,000 <63 <63 ********170 J **<33,000 <63 589 **160 J 120 J **1,280 339 <63* NR NR NR NR NR NR03/25/19 967 953 144 839 124 68.1 6,020 <5.0 ****809 <3.1 <3.1 ********51.1 **<1,600 5.1 J 71.3 **14.4 <3.1 **133 65.9 47.8*NR NR NR NR NR NR05/08/19 3,930 4,420 451 2,560 165 258 4,690 <0.20 ****710 <13 <13 ********63.5 **<6,500 20.7 J 156 **54.4 <13 **545 229 133*NR NR NR NR NR NR05/20/20 1,330 1,840 179 1,050 67.1 88.1 2,320 <10 ****680 <6.3 <6.3 ********26.6 **<3,300 6.8 J 66.4 **21.6 J <6.3 **217 137 35.4 *NR NR NR NR NR NR12/01/20 10,200 18,300 1,490 7,440 912 361 2,060 J <100 ****<1,000 <63 <63 ********123 J **<33,000 <63 386 **130 J 89.7 J **866 272 194 J*NR NR NR NR NR NR06/14/21 12,300 16,500 1,360 6,860 631 288 3,160 J NR <63 <63 <1,000 <63 <63 <63 <63 **<63 129 J <63 <33,000 <63 410 <63 100 J <63 <63 651 231 J 340*NR NR NR NR NR NR05/23/22 2,660 5230 791 3830 307 359 NR NR NR NR NR NR NR NR NR **<31 NR NR NR NR 144 NR NR NR NR NR NR NR NR NR NR NR NR NR06/21/22 6,280 13,500 E 1,450 7,150 <31 532 4,760 <20 <13 <13 <200 37.2 J 19.8 J <13 22.5 J 58.3 <13 39.4 J <13 <6500 60.4 199 <13 189 100 <13 1,930 443 105* NR NR NR NR NR NR02/23/23 5,230 9,000 1,230 5,530 158 427 2,050 <2.80 <1.60 <15.0 382 23.6 8.67 <1.90 <2.20 <2.20 <2.10 35.5 <1.90 <420 47.2 191 4.56 J 139 81.5 <2.70 905 293 101*NR NR NR NR NR NR09/26/17 1,050 115 225 1,500 290 40.8 NR NR ****NR <3.1 <3.1 ********68.9 **NR 10.5 J 364 **25.1 <3.1 **321 6.3 J 1.5 83.5 NR NR NR NR NR
10/25/18 241 26.5 54.3 376 95.7 10.9 1,160 3.1 J ****199 <0.63 <0.63 ********22.1 **<330 2.9 102 **6.8 <0.63 **83.6 0.94 J 0.62*NR NR NR NR NR NR01/07/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 ****<2.0 <0.13 <0.13 ********<0.13 **<65 <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 <0.13*NR NR NR NR NR NR
05/08/19 <0.13 <0.13 <0.13 <0.25 0.27 J <0.13 <2.0 <0.20 ****<2.0 <0.13 <0.13 ********0.15 J **<65 <0.13 0.36 J **<0.13 <0.13 **<0.13 <0.13 <0.13*NR NR NR NR NR NR05/20/20 2,190 3,030 291 1,630 85.0 128 2,250 <20 ****705 J <13 <13 ********32.8 J **<6,500 <13 86.2 **33.1 J <13 **316 183 54.9*NR NR NR NR NR NR12/01/20 628 42.0 112 911 504 41.5 2,390 15.0 J ****<50 <3.1 <3.1 ********52.9 **<1,600 6.5 J 253 **19.2 <3.1 **252 15.3 <3.1 *NR NR NR NR NR NR06/14/21 439 33.3 85.2 751 509 34.6 2,390 NR 10.9 3.7 J <40 <2.5 <2.5 6.7 J 112 **11.2 40.2 3.3 J <1,300 5.0 J 230 <2.5 13.0 <2.5 <2.5 175 9.3 J <2.5*NR NR NR NR NR NR06/21/22 291 252 66.8 547 337 257 1,690 <20 <13 <13 <200 <13 <13 <13 117 <20 <13 27.2 J <13 <6500 <13 163 <13 <13 <13 <13 187 30.4 J <13* NR NR NR NR NR NR02/23/23 95.1 22.1 19.7 212 207 9.45 1,100 7.84 J 5.03 <1.50 199 0.474 J 0.373 J 2.99 43.7 <0.220 5.77 13.3 1.63 <42.0 1.81 80.4 0.371 J 3.22 <0.220 <0.270 46.0 3.94 <0.200*NR NR NR NR NR NR11/30/17 47.8 0.26 J 0.79 16.3 <0.13 1.1 NR NR ****NR <0.13 <0.13 ********<0.13 **NR 0.61 <0.13 **0.98 <0.13 **<0.13 <0.13 0.034 416 NR NR NR NR NR06/14/21 14.3 <0.13 0.22 J 7.9 <0.13 1.0 2.8 J NR <0.13 <0.13 32.4 <0.13 <0.13 <0.13 <0.13 **<0.13 <0.13 <0.13 <65 0.28 J 0.19 J <0.13 0.45 J <0.13 <0.13 <0.13 0.45 J <0.13*NR NR NR NR NR NR06/21/22 10.2 <0.13 0.19 J 6.1 <0.13 1.2 <2.0 <0.20 <0.13 <0.13 59.1 <0.13 <0.13 <0.13 <0.13 <0.20 <0.13 <0.13 <0.13 <65 0.39 J 0.35 J <0.13 0.39 J <0.13 <0.13 <0.13 0.47 J <0.13*NR NR NR NR NR NR02/23/23 19.0 <0.220 0.648 8.80 <0.140 1.32 <1.90 <0.280 <0.160 <1.50 86.1 <0.180 <0.200 <0.190 <0.220 <0.220 <0.210 <0.150 <0.190 <42.0 0.533 <0.500 <0.089 0.533 <0.220 <0.270 <0.190 <0.180 <0.200*NR NR NR NR NR NR11/30/17 77.2 1.6 3.9 156 145 25.8 NR NR ****NR <0.25 <0.25 ********3.8 **NR 1.5 12.9 **0.91 J <0.25 **12.3 <0.25 0.11 38.3 NR NR NR NR NR06/14/21 5.1 0.17 J 0.91 25.2 49.8 3.3 58.0 NR <0.13 <0.13 <2.0 <0.13 <0.13 <0.13 0.87 **<0.13 1.3 <0.13 <65 0.25 J 4.9 <0.13 0.30 J <0.13 0.72 1.8 <0.13 <0.13*NR NR NR NR NR NR06/21/22 24.6 0.53 3.3 111 256 E 14.7 149 9.1 <0.13 <0.13 <2.0 0.30 J 0.31 J <0.13 3.9 0.71 0.25 J 3.0 <0.13 <65 1.9 15.0 0.19 J 2.0 <0.13 2.4 16.0 0.30 J <0.13* NR NR NR NR NR NR02/23/23 0.658 <0.220 0.597 6.00 57.6 1.15 <1.90 2.57 J <0.160 <1.50 55.3 <0.180 <0.200 <0.190 1.55 <0.220 <0.210 <0.150 <0.190 <42.0 <0.180 4.17 <0.089 <0.190 <0.220 <0.270 0.761 <0.180 <0.200*NR NR NR NR NR NR11/30/17 3.2 4.4 0.46 J 1.7 <0.13 <0.13 NR NR ****NR <0.13 <0.13 ********0.22 J **NR <0.13 0.19 J **<0.13 <0.13 **0.18 J <0.13 0.076 125 NR NR NR NR NR06/14/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 NM <0.13 <0.13 <2.0 <0.13 <0.13 <0.13 0.25 J **<0.13 <0.13 <0.13 <65 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13*NR NR NR NR NR NR02/23/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.50 <1.60 <0.180 <0.200 <0.190 <0.220 <0.220 <0.210 <0.150 <0.190 <42.0 <0.180 <0.500 <0.089 <0.190 <0.220 <0.270 <0.190 <0.180 <0.200*NR NR NR NR NR NR11/30/17 169 11.2 31.8 148 19.3 2.1 J NR NR ****NR <0.63 <0.63 ********15.5 **NR 1.3 J 69.1 **2.9 <0.63 **9.8 <0.63 0.31 314 NR NR NR NR NR10/25/18 48.3 2.1 11.5 54.6 16.6 1.6 403 0.44 J ****61.3 <0.25 <0.25 ********11.3 **<130 0.64 J 44.1 **1.2 <0.25 **5.9 <0.25 0.29 J*NR NR NR NR NR NR01/07/19 24.1 1.6 6.9 32.1 9.8 0.74 163 0.25 J ****25.0 <0.13 <0.13 ********7.3 **<65 0.39 J 31.3 **0.75 <0.13 **3.1 <0.13 <0.13*NR NR NR NR NR NR05/08/19 95.2 5.4 25.8 120 26.4 3.2 476 0.79 J ****83.8 0.26 J 0.21 J ********15.4 **<65 1.4 57.9 **3.0 <0.13 **14.4 <0.13 0.20 J*NR NR NR NR NR NR05/20/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 ****<2.0 <0.13 <0.13 ********<0.13 **<65 <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 <0.13 NR NR NR NR NR NR12/01/20 0.15 J 0.18 J <0.13 <0.25 1.8 <0.13 7.8 J <0.20 ****<2.0 <0.13 <0.13 ********1.6 **<65 <0.13 4.7 **<0.13 <0.13 **<0.13 <0.13 <0.13 *NR NR NR NR NR NR06/14/21 <0.13 <0.13 <0.13 <0.25 2.6 <0.13 5.3 J NR <0.13 <0.13 <2.0 <0.13 <0.13 <0.13 0.71 **<0.13 1.6 <0.13 <65 <0.13 1.6 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13*NR NR NR NR NR NR06/21/22 <0.13 <0.13 <0.13 <0.25 1.7 0.13 J <2.0 <0.20 <0.13 <0.13 <2.0 <0.13 0.35 J <0.13 0.45 J <0.20 <0.13 0.74 <0.13 <65 <0.13 0.97 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13* NR NR NR NR NR NR02/23/23 <0.180 <0.220 <0.170 <0.210 1.62 <0.470 <1.90 <0.280 <0.160 <1.50 <1.60 <0.180 <0.200 <0.190 1.02 <0.220 <0.210 <0.150 <0.190 <42.0 <0.180 1.53 <0.089 <0.190 <0.220 <0.270 <0.190 <0.180 <0.200*NR NR NR NR NR NR
MW-14
MW-12
MW-11
MW-10 C5-C8 AliphaticsC5- C8 Aliphatics (Unadj.)C9- C12 Aliphatics (Unadj.)C9-C12 AliphaticsMW-6 TolueneEthylbenzeneNaphthalene1,2,4-TrimethylbenzeneXylenesMTBEDi-isopropyl etherStyreneBromodichloromethaneBromoformDibromochloromethane(Chlorodibromomethane)TABLE 6SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTSKINGSWAY #10 (INCIDENT NO. 40626)
Analytical Method MADEP Method VPH
Facility ID # : 00-0-0000003687
EPA Methods 6200B and 602
1,2,3-TrichloropropaneC9-C10 Aromatics1,3,5-Trimethylbenzene1,2-Dibromoethane(EDB)Leadn-Propylbenzenesec-Butylbenzene1,2-DichloroethaneIsopropylbenzenen-Butylbenzene10 Times 2B Standards (µg/l)BenzeneMAC (µg/l)
GCL (µg/l)
Contaminant of Concern
Chloroform (Trichloromethane)p-Dichlorobenzene(1,4-Dichlorobenzene)1,2-Dichloropropanep-Isopropyltoluene(4-Isopropyltoluene)MW-5 Tert-Amyl AlcoholTert-Butyl Alcoholtert-Amyl methyl ether (TAME)MW-13
MW-3
MW-4
MW-1
MW-2
MW-9
MW-8
MW-7 Methyl Chloride (Chloromethane)EthanolPage 1 of 2
Date: 3/17/23
EPA
504.1
SW846
6010B
Well ID
Date
Collected(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 4 10 70 70 0.4 70 3 6 0.4 0.6 4,000 70 70 25 70 70 0.005 400 400 0.02 15 400 400 700 700 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 ######NE 4,000 10,000 5,900 8,800 400 70,000 3,000 405 400 600 4,000,000 30,500 70,000 11,700 26,100 70,000 NE 28,500 24,100 50 15,000 NE NE NE NE NE
510 110 1,300 6,700 15,000 120 NE NE 270 1,200 NE 39 NE 210 20,000 110,000 1,000 6,500 310 50,000 2,500 NE NE 800 NE 0.01 3,900 2,150 1 5.4 1,250 NE 1,800 NE 40,000C5-C8 AliphaticsC5- C8 Aliphatics (Unadj.)C9- C12 Aliphatics (Unadj.)C9-C12 AliphaticsTolueneEthylbenzeneNaphthalene1,2,4-TrimethylbenzeneXylenesMTBEDi-isopropyl etherStyreneBromodichloromethaneBromoformDibromochloromethane(Chlorodibromomethane)TABLE 6SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTSKINGSWAY #10 (INCIDENT NO. 40626)
Analytical Method MADEP Method VPH
Facility ID # : 00-0-0000003687
EPA Methods 6200B and 602
1,2,3-TrichloropropaneC9-C10 Aromatics1,3,5-Trimethylbenzene1,2-Dibromoethane(EDB)Leadn-Propylbenzenesec-Butylbenzene1,2-DichloroethaneIsopropylbenzenen-Butylbenzene10 Times 2B Standards (µg/l)BenzeneMAC (µg/l)
GCL (µg/l)
Contaminant of Concern
Chloroform (Trichloromethane)p-Dichlorobenzene(1,4-Dichlorobenzene)1,2-Dichloropropanep-Isopropyltoluene(4-Isopropyltoluene)Tert-Amyl AlcoholTert-Butyl Alcoholtert-Amyl methyl ether (TAME)Methyl Chloride (Chloromethane)Ethanol11/30/17 13,400 13,400 1,230 5,370 433 264 NR NR ****NR <63 <63 ********1,130 **NR <63 2,880 **86.9 J <63 **612 145 J 223 739 NR NR NR NR NR10/25/18 8,650 9,600 1,030 4,960 689 282 6,940 <40 ****1,630 J <25 <25 ********529 **<13,000 37.6 J 1,440 **113 <25 **767 133 114*NR NR NR NR NR NR01/07/19 6,500 8,270 926 4,480 724 208 4,880 <50 ****<500 <31 <31 ********391 **<16,000 31.7 J 1,180 **98.3 J <31 **613 103 J <31* NR NR NR NR NR NR05/08/19 7,400 8,170 970 4,530 906 268 8,740 <50 ****<500 <31 <31 ********474 **<16,000 36.6 J 1,330 **104 J <31 **681 136 129 J*NR NR NR NR NR NR05/20/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 ****<2.0 <0.13 <0.13 ********<0.13 **<65 <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 <0.13 NR NR NR NR NR NR12/01/20 9,450 10,500 1,190 5,910 1,390 251 4,610 <50 ****<500 <31 <31 ********354 **<16,000 <31 1,090 **110 J <31 **740 157 185*NR NR NR NR NR NR06/14/21 9,660 12,000 1,100 5,640 1,280 231 5,910 NR <31 <31 <500 <31 <31 <31 <31 **<31 468 <31 36,400 <31 1,550 <31 81.9 J <31 <31 547 130 221*NR NR NR NR NR NR06/21/22 7,100 8,160 899 4,390 1,150 534 4,280 <50 <31 <31 <500 <31 <31 <31 <31 67.3 J <31 253 <31 26,500 32.6 J 906 <31 95.0 J <31 <31 779 176 183* NR NR NR NR NR NR02/23/23 7,610 8,480 985 4,720 1,280 422 4,170 <28.0 <16.0 <150 1,350 <18.0 <20.0 <19.0 <22.0 <22.0 <21.0 199 <19.0 67,600 36.4 J 884 <8.90 104 <22.0 <27.0 694 231 <20.0*NR NR NR NR NR NR05/22/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR ****NR <0.13 <0.13 ********<0.13 **NR <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 0.20 <5.0 NR NR NR NR NR06/14/21 <0.13 <0.13 <0.13 <0.25 0.38 J <0.13 <2.0 NR <0.13 <0.13 <2.0 <0.13 <0.13 <0.13 <0.13 **<0.13 <0.13 <0.13 <65 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13*NR NR NR NR NR NR02/23/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.50 <1.60 <0.180 <0.200 <0.190 <0.220 <0.220 <0.210 <0.150 <0.190 <42.0 <0.180 <0.500 <0.089 <0.190 <0.220 <0.270 <0.190 <0.180 <0.200*NR NR NR NR NR NR05/22/18 <0.13 <0.13 <0.13 <0.25 <0.13 0.26 J NR NR ****NR <0.13 <0.13 ********<0.13 **NR <0.13 <0.13 **<0.13 <0.13 **0.42 J <0.13 <0.0095 <5.0 NR NR NR NR NR06/14/21 <0.13 0.38 J <0.13 <0.25 <0.13 0.21 J <2.0 NR <0.13 <0.13 <2.0 <0.13 <0.13 <0.13 <0.13 **<0.13 <0.13 <0.13 <65 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13*NR NR NR NR NR NR02/23/23 <0.180 2.21 <0.170 <0.210 <0.140 1.07 <1.90 <0.280 <0.160 <1.50 <1.60 <0.180 <0.200 <0.190 <0.220 <0.220 <0.210 <0.150 <0.190 <42.0 <0.180 <0.500 <0.089 <0.190 <0.220 <0.270 <0.190 <0.180 <0.200*NR NR NR NR NR NR05/22/18 <0.13 <0.13 <0.13 <0.25 <0.13 1.0 NR NR ****NR <0.13 <0.13 ********<0.13 **NR <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 <0.0095 5.2 NR NR NR NR NR06/14/21 <0.13 <0.13 <0.13 <0.25 <0.13 1.00 <2.0 NR <0.13 <0.13 3.3 J <0.13 <0.13 <0.13 <0.13 **<0.13 <0.13 <0.13 <65 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13*NR NR NR NR NR NR02/23/23 <0.180 <0.220 <0.170 <0.210 <0.140 2.77 <1.90 <0.280 <0.160 <1.50 <1.60 <0.180 <0.200 <0.190 <0.220 <0.220 <0.210 <0.150 <0.190 <42.0 <0.180 <0.500 <0.089 <0.190 <0.220 <0.270 <0.190 <0.180 <0.200*NR NR NR NR NR NR05/22/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR ****NR <0.13 <0.13 ********<0.13 **NR <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 <0.0095 <5.0 NR NR NR NR NR10/25/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 ****<2.0 <0.13 <0.13 ********<0.13 **<65 <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 0.23*NR NR NR NR NR NR01/07/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 ****<2.0 <0.13 <0.13 ********<0.13 **<65 <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 <0.13*NR NR NR NR NR NR
05/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 ****<2.0 <0.13 <0.13 ********<0.13 **<65 <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 <0.13*NR NR NR NR NR NR05/20/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 ****<2.0 <0.13 <0.13 ********<0.13 **<65 <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 <0.13 NR NR NR NR NR NR12/01/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 ****<2.0 <0.13 <0.13 ********<0.13 **<65 <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 <0.13 *NR NR NR NR NR NR06/14/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 NR <0.13 <0.13 <2.0 <0.13 <0.13 <0.13 <0.13 **<0.13 0.15 J <0.13 <65 <0.13 0.26 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13*NR NR NR NR NR NR02/23/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.50 <1.60 <0.180 <0.200 <0.190 <0.220 <0.220 <0.210 <0.150 <0.190 <42.0 <0.180 2.01 <0.089 <0.190 <0.220 <0.270 <0.190 <0.180 <0.200*NR NR NR NR NR NR05/26/17 6.0 3.3 0.77 1.7 <0.13 0.63 NR NR ****NR <0.13 <0.13 ********<0.13 **NR <0.13 <0.13 **0.16 J <0.13 **<0.13 <0.13 0.190 17.4 NR NR NR NR NR06/14/21 7.4 <0.13 <0.13 <0.25 0.28 J 2.6 33.9 NR 4.3 <0.13 85.2 <0.13 <0.13 1.2 9.8 **<0.13 0.29 J <0.13 <65 <0.13 2.4 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13* NR NR NR NR NR NR06/21/22 4.7 <0.13 <0.13 1.8 <0.13 3.7 78.2 <0.20 1.9 <0.13 216 <0.13 <0.13 0.50 4.2 <0.20 <0.13 0.47 J <0.13 <65 0.21 J 5.6 <0.13 <0.13 <0.13 <0.13 0.45 J 0.14 J <0.13* NR NR NR NR NR NR02/23/23 1.85 <0.220 0.460 J 0.501 <0.140 1.24 41.2 <0.280 <0.160 <1.50 135 <0.180 <0.200 <0.190 1.45 <0.220 <0.210 0.303 J <0.190 <42.0 <0.180 6.74 <0.089 <0.190 <0.220 <0.270 <0.190 <0.180 <0.200*NR NR NR NR NR NR04/13/20 9,130 27,100 2,570 13,500 283 J 633 NR NR ****NR NR NR ********NR **NR NR 314 J **NR NR **NR NR NR NR NR NR NR NR NR05/20/20 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP **FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP10/26/20 2,100 18,800 2,920 16,100 399 1,730 NR NR NR NR NR NR NR NR NR **<25 NR NR NR NR 154 J NR NR NR NR NR NR NR NR NR NR NR NR NR12/01/20 5,860 21,700 2,660 15,000 <63 837 <1,000 <100 ****<1,000 <63 <63 ********<63 **<33,000 75.1 J 142 J **229 J 94.1 J **2,310 539 68.9 J*NR NR NR NR NR NR05/10/21 1,130 8,250 1,010 6,720 275 901 NR NR NR NR NR NR NR NR NR **<25 NR NR NR NR 94.2 J NR NR NR NR NR NR NR NR NR NR NR NR NR06/14/21 4,070 20,200 2,380 13,800 <63 2,860 1,760 J NR <63 <63 <1,000 107 J <63 <63 <63 **<63 <63 <63 <33,000 65.0 J 116 J <63 316 <63 <63 3,180 704 <63*NR NR NR NR NR NR
06/21/22 1,360 13,100 E 2,640 14,400 E 283 1,760 3,360 <0.20 <0.13 <0.13 <2.0 37.3 17.6 <0.13 <0.13 32.7 <0.13 30.5 <0.13 <65 99.1 142 11.8 336 49.8 J 2.8 3,280 829 22.3*NR NR NR NR NR NR01/09/23 1,760 16,200 3,150 14,800 250 1,990 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR 128 NR NR NR NR NR NR NR NR NR NR NR NR NR02/23/23 6,800 25,400 2,380 14,400 <14.0 929 1,970 <28.0 <16.0 <150 <160 37.1 J <20.0 <19.0 <22.0 <22.0 <21.0 <15.0 <19.0 <4,200 81.5 191 <8.90 252 109 <27.0 2,220 634 <20.0*NR NR NR NR NR NR04/13/20 0.80 J 7.6 5.0 21.9 177 1.3 J NR NR ****NR NR NR ********NR **NR NR 40.4 **NR NR **NR NR NR NR NR NR NR NR NR05/20/20 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP **FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP10/26/20 <0.63 <0.63 <0.63 1.9 J 202 <0.63 NR NR NR NR NR NR NR NR NR **<0.25 NR NR NR NR 35.0 NR NR NR NR NR NR NR NR NR NR NR NR NR
12/01/20 17.9 102 82.2 339 264 48.2 916 11.7 ****500 3.2 1.4 ********6.8 **<160 6.6 44.8 **20.8 <0.31 **106 50.6 0.33 J*NR NR NR NR NR NR05/10/21 <0.25 0.35 J 0.61 J 3.5 160 <0.25 NR NR NR NR NR NR NR NR NR **<0.25 NR NR NR NR 13.4 NR NR NR NR NR NR NR NR NR NR NR NR NR
06/14/21 18.6 94.8 18.3 242 271 15.5 1,060 NR <1.3 <1.3 <20 <1.3 <1.3 <1.3 <1.3 **<1.3 5.4 <1.3 <650 <1.3 26.3 <1.3 3.4 J <1.3 <1.3 52.3 35.8 <1.3*NR NR NR NR NR NR06/21/22 <1.3 3.9 J 1.5 J 11.5 J 191 5.3 1,040 5.3 J <1.3 <1.3 845 <1.3 <1.3 <1.3 6.9 <2.0 <1.3 2.3 J <1.3 <650 <1.3 18.9 <1.3 <1.3 <1.3 <1.3 4.2 J 3.3 J <1.3* NR NR NR NR NR NR01/09/23 0.288 J 1.17 0.951 5.75 141 6.57 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR 18.3 NR NR NR NR NR NR NR NR NR NR NR NR NR02/23/23 6.51 64.4 17.0 236 90.4 12.1 187 3.55 J <0.160 <1.50 237 0.769 0.542 <0.190 5.47 <0.220 <0.210 <0.150 <0.190 <42.0 1.24 14.0 0.508 2.76 <0.220 <0.270 59.1 19.1 <0.200*NR NR NR NR NR NR05/23/22 12,800 15,900 1,570 7,530 571 735 NR NR NR NR NR NR NR NR NR **<130 NR NR NR NR 482 J NR NR NR NR NR NR NR NR NR NR NR NR NR06/21/22 1,100 2,530 381 1,979 145 114 488 10.8 <0.13 <0.13 <2.0 10.2 4.7 <0.13 <0.13 26.9 <0.13 18.7 <0.13 687 24.1 101 3.0 48.6 J 16.7 1.3 371 93.0 23.7*NR NR NR NR NR NR01/09/23 1,210 3,260 527 2,850 105 249 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR 78.0 NR NR NR NR NR NR NR NR NR NR NR NR NR02/23/23 1,030 3,110 564 2,740 91.8 211 635 <0.280 <0.160 <1.50 608 J 9.87 4.37 <0.190 <0.220 <0.220 <0.210 14.9 <0.190 <42.0 28.9 63.9 2.82 86.0 24.3 <0.270 621 155 16.5*NR NR NR NR NR NR05/26/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR ****NR <0.13 <0.13 ********<0.13 **NR <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 NR NR NR NR NR NR NR09/26/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR ****NR <0.13 <0.13 ********<0.13 **NR <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 NR NR NR NR NR NR NR05/02/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR ****NR <0.13 <0.13 ********<0.13 **NR <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 NR NR NR NR NR NR NR05/22/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR ****NR <0.13 <0.13 ********<0.13 **NR <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 NR NR NR NR NR NR NR10/25/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR ****NR <0.13 <0.13 ********<0.13 **NR <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 NR NR NR NR NR NR NR01/07/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR ****NR <0.13 <0.13 ********<0.13 **NR <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 NR NR NR NR NR NR NR03/25/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR ****NR <0.13 <0.13 ********<0.13 **NR <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 NR NR NR NR NR NR NR05/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR ****NR <0.13 <0.13 ********<0.13 **NR <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 NR NR NR NR NR NR NR04/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR ****NR NR NR ********NR **NR NR <0.13 **NR NR **NR NR NR NR NR NR NR NR NR05/20/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR ****NR <0.13 <0.13 ********<0.13 **<65 <0.13 <0.13 **<0.13 <0.13 **<0.13 <0.13 <0.13 NR NR NR NR NR NR12/01/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR NR <2.0 <0.13 <0.13 NR NR **<0.13 <0.13 NR <65 <0.13 <0.13 NR <0.13 <0.13 NR <0.13 <0.13 <0.13 *NR NR NR NR NR NR05/10/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR NR NR NR NR **<0.25 NR NR NR NR <0.13 NR NR NR NR NR NR NR NR NR NR NR NR NR06/14/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 NR <0.13 <0.13 <2.0 <0.13 <0.13 <0.13 <0.13 **<0.13 <0.13 <0.13 <65 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13*NR NR NR NR NR NR05/23/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR NR NR NR NR **<0.13 NR NR NR NR <0.13 NR NR NR NR NR NR NR NR NR NR NR NR NR06/21/22 <0.13 <0.13 <0.13 NM <0.13 <0.13 <2.0 <0.20 <0.13 <0.13 <2.0 <0.13 <0.13 <0.13 <0.13 <0.20 <0.13 <0.13 <0.13 <65 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13* NR NR NR NR NR NR01/09/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR <0.500 NR NR NR NR NR NR NR NR NR NR NR NR NR02/23/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 NA NA <0.160 <1.50 NA <0.180 <0.200 <0.190 <0.220 <0.220 <0.210 <0.150 <0.190 <42.0 <0.180 <0.500 <0.089 <0.190 <0.220 <0.270 <0.190 <0.180 <0.200*NR NR NR NR NR NR
Notes:• Results reported in micrograms per liter (µg/l).• < : Less than the method detection limit specified in the laboratory report.• *: EDB results from Method 6200B analysis.• **: Concentrations from prior detections have not been updated.• NR: Not Requested.• NM: Not Measured.• E: Indicates value exceeds calibration range.• Refer to laboratory report for detected constituents that did not exceed the MACs, or for which no standard has been established.
• Area of the contaminant plume is calculated from Figure #6.
MW-15
Trip Blank
RW-3
RW-2
RW-1
TW-1
• Other reported compounds above the MACs: 5/26/17: chloroform, bromodichloromethane, bromoform, dibromochloromethane, 1,4-dichlorobenzene, 1,2-dichloropropane and tetrachloroethene in MW-5, bromodichloromethane and dibromochloromethane in TW-1; 9/26/17: chloroform, bromodichloromethane, methylchloride and methylene chloride in MW-10;
11/30/17: bromodichloromethane and dibromochloromethane in MW-13; 10/25/18: chloroform in MW-2 and MW-9, bromodichloromethane in MW-10; 03/25/19: 1,4-Dichlorobenzene and Methylene Chloride in MW-2; 05/05/20: Methyl Chloride in MW-14 and MW-19; 12/01/20: bromodichloromethane, chloroform and dibromochloromethane in MW-10, 1,2,3-
trichloropropane in RW-2; 6/21/22: methyl chloride, o-chlorotoluene, EDB, o-dichlorobenzene, methylene chloride, and/or 1,1,2,2-tetrachloroethane in MW-1, MW-5, MW-9, MW-10, MW-12, MW-15, RW-1, RW-2, and RW-3; 2/13/23: 1,1,2,2-tetrachloroethane in MW-9;
MW-17
MW-18
MW-19
MW-16
Page 2 of 2
Date: 03/17/23 Facility ID#: 00-0-0000003687
Method of Measurement:Interface probe at top-of-casing
Well ID Product Type
(gas, diesel, etc.)
Date of
Recovery
(mm/dd/yy)
Free Product
Recovery
Method*
Casing
Diameter
(inches)
Product Thickness
before Recovery
(feet)
Product Thickness
after Recovery
(feet)
Amount of Liquid
Recovered
(gallons)
Amount of
Product
Recovered
(gallons)
MW-2 Gasoline 09/26/17 Hand Bailing 2 0.19 0.00 2.04 0.04
MW-1 1.47 0.00
MW-2 0.04 0.00
MW-9 0.00 0.00
MW-1 0.90 0.00
MW-2 0.00 0.00
MW-9 0.00 0.00
MW-1 0.00 0.00
MW-2 0.00 0.00
MW-9 0.00 0.00
RW-1 0.00 0.00
RW-2 0.00 0.00
RW-1 0.00 0.00
RW-2 0.00 0.00
RW-1 0.00 0.00
RW-2 0.00 0.00
MW-9 2 0.00 0.00
RW-3 4 0.00 0.00
MW-2 2 0.03 0.00
RW-1 0.00 0.00
RW-2 0.00 0.00
RW-3 0.00 0.00
Notes :
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Liquid Recovered (gallons) includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
2 2,423
0.00Gasoline 04/13/20 to
04/17/20 MMPE 4 1,659
TABLE 7
FREE PRODUCT RECOVERY RESULTS
KINGSWAY #10 (INCIDENT NO. 40626)
Gasoline 11/20/17 AFVR 2 1,145 0.00
0.00
0.00
0.00
Gasoline 05/02/18 AFVR 2 838
Gasoline 03/25/2019
to 03/29/19
Gasoline 10/26/20 to
10/30/20 MMPE 4 4,860
MMPE
• Amount of Product Recovered (in gallons) includes only the volume of free product in the tanker at the end of the event (based on Disposal Manifest and/or
field notes).
0.00Gasoline 05/10/21 to
05/14/21 MMPE 4 4,770
Gasoline 5/23/22 to
5/27/22 MMPE 4,980 0.00
Gasoline 1/09/23 to
1/13/23 MMPE 4 0.00
0.00
3,685
5,810
Page 1 of 1
Date: 03/17/23 Facility ID #: 00-0-0000003687
MW-2 09/26/17 Hand Bailing ---------0.00 2.04 0.04 0.04
MW-1
MW-2
MW-9
MW-1
MW-2
MW-9
MW-1
MW-2
MW-9
RW-1
RW-2
RW-1
RW-2
RW-1
RW-2
MW-9
RW-3
MW-2
RW-1
RW-2
RW-3
1018.69 30,172.04 0.04 1,018.73
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Vaporized Product (in gallons) is based on Vapor Emissions Summary Sheet, = total emissions in pounds/6.15
• Amount of Liquid Recovered includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered as Liquid includes only the volume of free product in the tanker at the end of the event (based on Disposal
Manifest and/or Field Notes).
• Total Amount of Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Total Fluids Removed = Amount of Vaporized Product + Amount of Liquid Recovered
• Information regarding historical free product recovery activities is not available.
Total To Date 31,190.73 1,018.73
0.1805/02/18 AFVR 1,333.57 133.50 273.50
3.60 2,423 0.00 3.60
03/25/19 to
03/29/19 MMPE 4,435.22 59.85 265.94
10/26/20 to
10/30/20 593.410.004,860593.4162,444.44
838 0.00 0.18
Totals
SUMMARY OF FLUID REMOVAL
Summary Total Fluids Removed (in gallons)Total Product Removed (in gallons)
Current Event 9,515.44 20.44
113.331,500.00MMPE
177.68 4,980 0.00 177.68
05/23/22 to
05/27/22 MMPE 1,364 119.44 4,750
04/13/20 to
04/17/20 MMPE 3,338.89 133.55 89,666.67 197.63 1,659 0.00 197.63
11/20/17 AFVR 1,705.14 151.43 1,198.76 0.95 1,145 0.00 0.95
TABLE 8
FREE PRODUCT RECOVERY EVENT INFORMATION
KINGSWAY #10 (INCIDENT NO. 40626)
Well ID Date
(mm/dd/yy)
Product
Recovery
Method*
Average
Effluent
Velocity
(ft/min)
Average
Effluent
Temperature
(°F)
Average
Effluent
Concentration
(ppm)
Amount of
Vaporized
Product
(gallons)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid
(gallons)
Total Amount
of Product
Recovered
(gallons)
24.80 4,770 0.00 24.80
05/10/21 to
05/14/21 MMPE 1,271 141.22 3,272.22
1,100 0.00
0.003,685
5,810
20.4401/09/23 to
01/13/23 MMPE
3,644 116.78 833 2.17
18.272,667120.44
Page 1 of 1
Date: 03/27/23 Facility ID #: 00-0-0000003687
Wells
Included in
Event
Product
Recovery
Method*
Date of Event
(mm/dd/yy)
Total Amount of Free
Product plus Ground
Water Recovered
(gallons)
Cost of Free
Product
Recovery Event
Cost Per Gallon
(total liquids)
MW-2 Hand Bailing 09/26/17 2.04 $555.00 $272.06
MW-1,
MW-2 and
MW-9
AFVR 11/20/17 1,145.95 $2,714.75 $2.37
MW-1,
MW-2 and
MW-9
AFVR 05/02/18 838.18 $2,607.30 $3.11
MW-1,
MW-2 and
MW-9
MMPE 03/25/19 to
03/29/19 2,426.60 $9,648.05 $3.98
RW-1 and
RW-2 MMPE 04/13/20 to
04/17/20 1,856.63 $8,888.01 $4.79
RW-1 and
RW-2 MMPE 10/26/20 to
10/30/20 9,515.44 $10,145.45 $1.07
RW-1 and
RW-2 MMPE 5/10/21 to
5/14/21 4,794.80 $10,102.11 $2.11
MW-9 and
RW-3 MMPE 5/23/22 to
5/27/22 5,157.68 $8,610.23 $1.67
MW-2, RW-
1, RW-2,
and RW-3
MMPE 01/09/23 to
01/13/23 9,513.27 $18,574.75 $1.95
35,250.59 $71,845.65 $2.04
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Total Amount of Free Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Cost of Free Product Recovery Event includes supervision, travel, mileage, per diem, subcontractor costs, MMPE sampling, MMPE sampling analytical, report
preparation (pre-2015 only) and project management.
Cost per gallon for the event is based on a total volume of
1,856.63 gallons of free product and water.
TOTAL (to date)
Cost per gallon for the event is based on a total volume of
838.18 gallons of free product and water.
TABLE 9
FREE PRODUCT RECOVERY COST SUMMARY
KINGSWAY #10 (INCIDENT NO. 40626)
Comments
---
Cost per gallon for the event is based on a total volume of
1,145.95 gallons of free product and water.
Cost per gallon for the event is based on a total volume of
2,426.60 gallons of free product and water.
Cost per gallon for the event is based on a total volume of
1,856.63 gallons of free product and water.
Cost per gallon for the event is based on a total volume of
4,770 gallons of free product and water.
Cost per gallon for the event is based on a total volume of
4,980 gallons of free product and water.
Cost per gallon for the event is based on a total volume of
9,495 gallons of free product and water.
Page 1 of 1

APPENDICES

APPENDIX A
State Correspondence

August 12, 2022 Kingsway Enterprises, Inc.
407 South Marietta Street Gastonia, North Carolina 28052 Attention: Mark King
Re: Notice of Regulatory Requirements 15A NCAC 2L .0407 Kingsway #10 1418 West Garrison Boulevard, Gastonia Gaston County Incident Number: 40626 Risk Classification: Intermediate Dear Mr. King:
The Groundwater Monitoring Report was received by the Division of Waste Management’s Underground Storage Tank Section, Mooresville Regional Office, on August 1, 2022. The report has been reviewed and will remain in the UST Section’s files. Upon review, the Division agrees with your consultant’s recommendation to conduct another MMPE prior
to the next scheduled groundwater sampling event, which should be conducted in December 2022, with the results received no later than January 31, 2023. If possible, this MMPE event should utilize all three recovery wells, RW-1, RW-2, and RW-3. In addition, as monitoring well MW-15 is not accessible for active remediation, the use of chemical or microbial
injection at MW-15 should be considered and, if feasible, implemented. If you have any questions regarding the actions that must be taken, or the rules mentioned in this letter, please contact me at the address or telephone number listed below for the Mooresville Regional Office. Sincerely, Brad C. Newton, P.G.
Hydrogeologist Mooresville Regional Office UST Section, Division of Waste Management, NCDEQ
cc: Joanna Alley – Geologic Resources, Inc. (via e-mail) Gaston County Health Department
4187 Received AUG 12 2022
Site Name City / County /Gaston Incident #40626
Resp Pty Name / Contact Incident Mgr Region MORRP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #14
Consultant / Project Mgr /Joanna R Alley
Telephone / Fax Number /Task Authorization Number:15 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:I130D RRA Date:
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
 Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.3rd Pty Ded?Task #Lab /
SubCode RO AuthProposed
Rate/Price
(Consultant)CO AuthProposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
4.031 26 /wells y $110.00 y $2,860.00 $2,860.00 /
4.090 #220 4 /samples y $40.00 y $160.00 $160.00 /
4.090 #240 23 /samples y $94.00 y $2,162.00 $2,162.00 /
4.090 #272 1 /sample y $66.00 y $66.00 $66.00 /
4.091 2 /shipments y $60.00 y $120.00 $120.00 /
6.090 1 /report y $1,125.00 y $1,125.00 $1,125.00 /
7.201 8 /hours y $93.00 y $744.00 $744.00 /
7.420 2 /events y $2,325.00 y $4,650.00 $4,650.00 /
7.420 2 /events y $1,500.00 y $3,000.00 $3,000.00 /
7.420 2 /events y $2,500.00 y $5,000.00 $5,000.00 /
7.420 5000 /gallons y $0.35 y $1,750.00 $1,750.00 /
7.420 5000 /gallons y $0.25 y $1,250.00 $1,250.00 /
12.030 4 /nights y $151.00 y $604.00 $604.00 /
12.050 3 /trips y $250.00 y $750.00 $750.00 /
12.055 3 /trips y $50.00 y $150.00 $150.00 /
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed 3
TOTAL:$24,391.00 $24,391.00 TOTAL:
Total Standard Costs (Not Third Party)$24,391.00 $24,391.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty CostsProcess Tracking (Date)
TA Submittal:9/26/22 by:(PM)(Reserved for RO)
RO Review:10/13/22 by:(IM)Joint UST Preapproval Confirmed By:Date1 10/21/2022
CO Review:10/21/22 by:(STF)RP or Designee Receipt Confirmation By:Date 4
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee and returned to the Trust Fund within a week of approval. Signature
indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work proceeding. Scope/costnegotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the UST Section and RPis not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 4/1/2022
JRA
Proposed
Units / Type
(Consultant)
Brad Newton
YES22-576 Nov. - Dec. 2022
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
FINAL REIMBURSEMENT
[e-mail]
Kingsway Enterprises, Inc.Mark King
Geological Resources, Inc.
DIRECTED COSTS
Gastonia
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010 (Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Kingsway 10
Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If,following completion of this ePATA,
you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATA requestdesignated as a "Change Order" in the provided space above prior to conducting those tasks.Include a copy of the prior ePATA form for confirmation.Please attach this form to
the cover of the corresponding claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12months ofthe completion date of the FIRST completed task to remain within the Statute ofLimitations.All ePATAs submitted withina claim areclosed with that
claim,and may not be re-used in a separate submittal,even for costs or tasks that were not originally claimed.Final reimbursement of costs associated with the Total Claimedamount below may be affected by the eligibility status of the site (i.e.,deductibles,apportionment,etc.),and the documentary validation of incurred costs as reasonable and
necessary expenses per 15A NCAC 2P .0402 and .0404.
bcn
HB
(Initials)
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORMDept of Environmental Quality -Division of Waste Management
10/21/22
4187 received OCT 24 2022

APPENDIX B
Land Use Information
Date: 03/30/23 Facility ID # : 00-0-0000005620
Map ID No.Land Use Feature Zoning Description Address
Distance from
Source Area
(feet)
1 Boys & Girls Clubs of Gaston RS-8 Community Center 399 S Boyd St
Gastonia, NC 28052 ~1,450 E
2 Gastonia Optimist Club Park RS-8 Park 403 S Vance St
Gastonia, NC 28052 ~1,450 E
3 Full Gospel UMU Church 1315 W 2nd Ave
Gastonia, NC 28052 ~950 NE
4 Blessed Assurance Outreach
Ministry I-U Church 1236 W 2nd Ave
Gastonia, NC 28052 ~1,500 NE
5 Faith Hope Love Apostolic
Church of Jesus Christ I-U Church 308 Linwood Rd
Gastonia, NC 28052 ~400 N
n/a C-1 Highway Commercial n/a n/a
n/a C-3 General Commercial n/a n/a
n/a C-3 CD General Commercial -
Conditional Zoning n/a n/a
n/a I-U Urban Industrial n/a n/a
n/a I-1 CD Light Industrial -
Conditional Zoning n/a n/a
n/a O-1 Office n/a n/a
n/a RMF Multi-family residential n/a n/a
n/a RS-8 Single-family residential n/a n/a
n/a UMU Urban Mixed Use n/a n/a
Note:
• Properties are keyed to Figure 3B.
APPENDIX B
LAND USE INFORMATION
KINGSWAY #10 (INCIDENT NO. 40626)
Page 1 of 1

APPENDIX C
NCDEQ Incident Report
NCDEQ Incident Report
RP/Company KINGSWAY ENTERPRISES, INC.
RPAddress 901 NORTH MARIETTA STREET
RPCity GASTONIA
Contact MARK KING
RPState NC
TELEPHONE [phone]
IncidentNumber 40626 USTNum MO-9144
IncidentName KINGSWAY 10
FacilID 00-0-0000003687
Address 1418 WEST GARRISION BOULEVARD
CityTown GASTONIA State NC
ZipCode
DateOccurred 5 /26/2016
DateReported 6 /24/2016
ConfRisk I
CloseOut
COMMENT
RptType Rcvd Rvwd Appvd
Incident Mgr BCNLongitude-81.207308 Latitude 35.257947
County GASTO
LSA1 1/9/2017 1/27/2017 1/27/2017
OTH 10/12/2017 10/27/2017 10/27/2017
FREE PRODUCT EVALUATION
FPRI 12/18/2017 1/12/2018 1/12/2018
FPRS 5/21/2018 6/6/2018 6/6/2018
CSAS 7/25/2018 8/8/2018 8/9/2018
Tuesday, March 21, 2023 Page 1 of 2
RMR 11/19/2018 12/12/2018 12/12/2018
RMR 2/6/2019 2/20/2019 2/20/2019
a sheen of free product was reported in monitoring wells MW-1 and MW-
2. therefore, gw samples should not have been collected from these two
wells.
RMR 6/6/2019 6/17/2019 6/17/2019
RMR 6/16/2020 6/25/2020 6/25/2020
RMR 2/1/2021 2/17/2021 2/17/2021
RMR 8/16/2021 8/25/2021 8/25/2021
RMR 8/1/2022 8/12/2022 8/12/2022
Tuesday, March 21, 2023 Page 2 of 2
NCDEQ Incident Report
RP/Company
RPAddress 3562 FIELDSTONE DRIVE
RPCity GASTONIA
Contact NATVARLAL PATEL
RPState NC
TELEPHONE
IncidentNumber 47766 USTNum MO-28514
IncidentName OMNI MART 33
FacilID 00-0-0000001144
Address 401 SOUTH LINWOOD ROAD
CityTown GASTONIA State NC
ZipCode 28052-
DateOccurred 4 /15/2021
DateReported 5 /6 /2021
ConfRisk L
CloseOut 1/7/2022
COMMENT
RptType Rcvd Rvwd Appvd
Incident Mgr BCNLongitude-81.207788 Latitude 35.257398
County GASTO
SCH 5/6/2021 5/17/2021 5/17/2021
Tuesday, March 28, 2023 Page 1 of 1

APPENDIX D
Historical Soil Quality Information
Date: 05/29/18
→5030/
8015C
50 NE NE NE NE NE NE NE NE NE NA NE NE NE NE NE
NE 0.0056 4.3 4.9 4.6 0.091 0.16 4.3 1.7 1.7 1.5 8.5 8.3 68 540 31
NE 18 1,200 1,560 3,129 350 313 626 1,564 626 3,128 782 782 939 1,500 469
SB-R2 FILL PORT (3') 05/26/16 Spill Bucket 3 7.44 J NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SB-2 (3') 08/16/16 Spill Bucket 3 <4.2 <0.0017 0.0022 J 0.0052 J 0.0269 NR NR NR NR NR NR NR NR NR NR NR
SB-3 (3') 08/16/16 Spill Bucket 3 16.7 0.0395 0.0351 0.460 1.55 NR NR NR NR NR NR NR NR NR NR NR
MW-1 (10') 12/13/16 Spill Bucket 10 NR <0.094 0.641 2.21 18.2 0.0841 J 28.1 3.94 0.883 3.40 <0.075 53.2 11.5 46.1 245 315
MW-1 (20') 12/13/16 Spill Bucket 20 NR 1.03 51.5 60.5 367 0.293 J 67.2 18.0 9.43 39.8 1.12 243 75.3 1,190 1,220 1,710
DI-1 (5') 09/18/17
Dispenser
Island 5 NR 0.0076 0.0067 B 0.0026 J 0.0123 J 0.0017 J 0.0040 J <0.0012 <0.0012 <0.0012 <0.0012 0.0053 J 0.0021 J <2.5 <2.5 <2.5
DI-2 (5') 09/18/17
Product
Piping 5 NR 0.124 J 7.52 B 18.9 114 <0.064 10.9 2.64 1.99 9.03 <0.064 70.9 21.3 489 <21 269 J
DI-3 (5') 09/18/17
Dispenser
Island 5 NR 0.0097 0.0176 B 0.0038 J 0.0360 <0.0011 <0.0021 <0.0011 <0.0011 <0.0011 <0.0011 0.0065 0.0019 J <2.3 <2.3 <2.3
DI-4 (5') 09/18/17
Product
Piping 5 NR 0.0032 J 0.0013 JB <0.0010 <0.0022 <0.0010 <0.0021 <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <2.5 <2.5 <2.5
DI-5 (5') 09/18/17
Dispenser
Island 5 NR 0.0409 <0.0014 <0.0014 <0.0029 0.0042 J <0.0027 <0.0014 <0.0014 <0.0014 <0.0014 <0.0014 <0.0014 <3.0 <3.0 <3.0
PP-1 (5') 09/18/17
Product
Piping 5 NR 0.0188 0.0097 B 0.0056 J 0.0194 0.0050 J <0.0025 <0.0012 <0.0012 0.0015 J <0.0012 0.0040 J <0.0012 <2.5 <2.5 <2.5
PP-2 (5') 09/18/17
Product
Piping 5 NR 0.0280 0.0093 B 0.0082 0.0161 J 0.0075 0.0038 J <0.0012 0.0016 J 0.0034 J <0.0012 0.0064 0.0015 J 4.66 J <3.0 <3.0
SB-1 (15') 09/18/17 UST Basin 15 NR 0.0161 0.0828 B 0.0375 0.315 0.0946 0.889 0.0147 0.0123 0.0197 <0.0015 0.269 0.0802 4.22 J <3.1 5.37 J
SB-2 (15') 09/18/17 UST Basin 15 NR <0.0020 <0.0016 <0.0016 <0.0034 <0.0016 <0.0032 <0.0016 <0.0016 <0.0016 <0.0016 <0.0016 <0.0016 <2.9 <2.9 <2.9
SB-3 (15') 09/18/17 UST Basin 15 NR <0.0019 <0.0016 <0.0016 <0.0033 0.0016 J <0.0031 <0.0016 <0.0016 <0.0016 <0.0016 <0.0016 <0.0016 <2.8 <2.8 <2.8 C9-C10 Aromaticsn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC9-C12 AliphaticsSoil-to-Water MCCs (mg/kg)
Residential SCLs (mg/kg)
RAL (mg/kg)Sample IDDate Collected (mm/dd/yy)Sample LocationSample Depth (ft-BGS)XylenesEPA Methods 8260B
TABLE 4
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
KINGSWAY #10 (INCIDENT NO. 40626)Naphthalene MTBEn-ButylbenzeneStyreneFacility ID # : 00-0-0000003687
Gasoline-Range TPH Analytical Method BenzeneTolueneEthylbenzeneMADEP Method VPH
IsopropylbenzenePage 1 of 2
Date: 05/29/18
→5030/
8015C
50 NE NE NE NE NE NE NE NE NE NA NE NE NE NE NE
NE 0.0056 4.3 4.9 4.6 0.091 0.16 4.3 1.7 1.7 1.5 8.5 8.3 68 540 31
NE 18 1,200 1,560 3,129 350 313 626 1,564 626 3,128 782 782 939 1,500 469C9-C10 Aromaticsn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC9-C12 AliphaticsSoil-to-Water MCCs (mg/kg)
Residential SCLs (mg/kg)
RAL (mg/kg)Sample IDDate Collected (mm/dd/yy)Sample LocationSample Depth (ft-BGS)XylenesEPA Methods 8260B
TABLE 4
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
KINGSWAY #10 (INCIDENT NO. 40626)Naphthalene MTBEn-ButylbenzeneStyreneFacility ID # : 00-0-0000003687
Gasoline-Range TPH Analytical Method BenzeneTolueneEthylbenzeneMADEP Method VPH
IsopropylbenzeneSB-4 (15') 09/18/17 UST Basin 15 NR 0.0086 J <0.0021 <0.0021 <0.0043 <0.0021 <0.0041 <0.0021 <0.0021 <0.0021 <0.0021 <0.0021 <0.0021 <2.7 <2.7 <2.7
SB-5 (15') 09/18/17 UST Basin 15 NR <0.11 <0.088 <0.088 <0.18 <0.088 <0.18 <0.088 <0.088 <0.088 <0.088 0.289 J <0.088 4.36 J <3.5 <3.5
SB-6 (15') 09/18/17 UST Basin 15 NR 0.0268 0.0021 JB 0.0183 0.0352 0.0117 <0.0026 <0.0013 0.0018 J 0.0045 J <0.0013 0.0289 0.0106 <2.8 <2.8 <2.8
SB-7 (15') 09/18/17 UST Basin 15 NR 0.0410 0.0088 JB 0.0411 0.119 0.0059 J 0.0072 J 0.0038 J 0.0054 J 0.0154 <0.0026 0.120 0.0395 <4.2 <4.2 <4.2
SB-8 (5') 09/18/17
Product
Piping 5 NR <0.0015 <0.0012 <0.0012 <0.0025 0.0026 J <0.0024 <0.0012 <0.0012 <0.0012 <0.0012 <0.0012 <0.0012 <2.9 <2.9 <2.9 Notes:
• Results reported in mg/kg.
• ft-BGS: feet below ground surface.
• RAL: Regulatory Action Level.
• MCCs: Maximum Contaminant Concentrations (soils).
• SCLs: Soil Cleanup Levels.
• <: Less than the method limit specified in the laboratory report.
• J: Estimated value.
• B: Analyte found in associated method blank.
• NE: Not Established.
• NR: Not Requested.
• Concentrations in bold face type exceed the RALs and/or the soil-to-water MCCs.
• Concentrations in italics face type exceed the Residential SCLs.
Page 2 of 2

APPENDIX E
Laboratory Analytical Reports

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

1/24/2023
Geological Resources, Inc. Joanna Alley
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-011-0102 Client Project Description: Kingsway #10
GRI # 5351
Dear Joanna Alley:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/11/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 14
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-011-0102
Page 2 of 14
Report Number:
Sample Summary Table
Client Project Description:
23-011-0102
Kingsway #10
GRI # 5351
Lab No Client Sample ID Matrix Date Collected Date Received
01/09/2023 09:52Aqueous 97293 RW-1 01/11/2023 15:04
01/09/2023 09:35Aqueous 97294 RW-2 01/11/2023 15:04
01/09/2023 09:20Aqueous 97295 RW-3 01/11/2023 15:04
01/09/2023Aqueous 97296 Trip Blank 01/11/2023 15:04
Page 3 of 14
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-011-0102
Report Limit
Project:Kingsway #10
V 97293RW-1
1760 01/21/2023 21:176200BBenzeneµg/L 180
128 01/19/2023 09:506200BDi-Isopropyl Ether (DIPE)µg/L 5.00
3150 01/21/2023 21:176200BEthylbenzeneµg/L 170
250 01/19/2023 09:506200BMethyl tert-butyl ether (MTBE)µg/L 1.40
1990 01/21/2023 21:176200BNaphthaleneµg/L 470
16200 01/21/2023 21:176200BTolueneµg/L 220
4680 01/21/2023 21:176200Bo-Xylene µg/L 210
10100 01/21/2023 21:176200Bm,p-Xylene µg/L 420
14800 01/21/2023 21:176200BXylene (Total)µg/L 210
V 97294RW-2
J0.288 01/19/2023 08:346200BBenzeneµg/L 0.180
18.3 01/19/2023 08:346200BDi-Isopropyl Ether (DIPE)µg/L 0.500
0.951 01/19/2023 08:346200BEthylbenzeneµg/L 0.170
141 01/21/2023 18:226200BMethyl tert-butyl ether (MTBE)µg/L 1.40
6.57 01/19/2023 08:346200BNaphthaleneµg/L 0.470
1.17 01/19/2023 08:346200BTolueneµg/L 0.220
2.45 01/19/2023 08:346200Bo-Xylene µg/L 0.210
3.30 01/19/2023 08:346200Bm,p-Xylene µg/L 0.420
5.75 01/19/2023 08:346200BXylene (Total)µg/L 0.210
V 97295RW-3
1210 01/21/2023 20:526200BBenzeneµg/L 18.0
78.0 01/19/2023 10:156200BDi-Isopropyl Ether (DIPE)µg/L 5.00
527 01/19/2023 10:156200BEthylbenzeneµg/L 1.70
105 01/19/2023 10:156200BMethyl tert-butyl ether (MTBE)µg/L 1.40
249 01/19/2023 10:156200BNaphthaleneµg/L 4.70
3260 01/21/2023 20:526200BTolueneµg/L 22.0
864 01/19/2023 10:156200Bo-Xylene µg/L 2.10
1990 01/19/2023 10:156200Bm,p-Xylene µg/L 4.20
2850 01/19/2023 10:156200BXylene (Total)µg/L 2.10
Page 4 of 14
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0102
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI # 5351 Received : 01/11/2023
Kingsway #10
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:RW-1
97293 Matrix:
1/9/2023 9:52
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00 V29072 01/21/23 09:00
1760 µg/L 180 500Benzene 1000 01/21/23 21:17 V29073MSA
128 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 01/19/23 09:50 V29021MSA
3150 µg/L 170 500Ethylbenzene 1000 01/21/23 21:17 V29073MSA
250 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 01/19/23 09:50 V29021MSA
1990 µg/L 470 1000Naphthalene 1000 01/21/23 21:17 V29073MSA
16200 µg/L 220 500Toluene 1000 01/21/23 21:17 V29073MSA
4680 µg/L 210 500o-Xylene 1000 01/21/23 21:17 V29073MSA
10100 µg/L 420 1000m,p-Xylene 1000 01/21/23 21:17 V29073MSA
14800 µg/L 210 500
Xylene (Total)1000 01/21/23 21:17 V29073
Surrogate: 4-Bromofluorobenzene 92.2 Limits: 70-130%01/19/23 09:5010 MSA V29021
Surrogate: Dibromofluoromethane 95.8 Limits: 70-130%01/19/23 09:5010 MSA V29021
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%01/19/23 09:5010 MSA V29021
Surrogate: Toluene-d8 99.6 Limits: 70-130%01/19/23 09:5010 MSA V29021
Surrogate: 4-Bromofluorobenzene 105 Limits: 70-130%01/21/23 21:171000 MSA V29073
Surrogate: Dibromofluoromethane 96.4 Limits: 70-130%01/21/23 21:171000 MSA V29073
Surrogate: 1,2-Dichloroethane - d4 97.4 Limits: 70-130%01/21/23 21:171000 MSA V29073
Surrogate: Toluene-d8 102 Limits: 70-130%01/21/23 21:171000 MSA V29073
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 5 of 14
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0102
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI # 5351 Received : 01/11/2023
Kingsway #10
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:RW-2
97294 Matrix:
1/9/2023 9:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00 V29072 01/21/23 09:00
0.288 J µg/L 0.180 0.500Benzene 1 01/19/23 08:34 V29021MSA
18.3 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 01/19/23 08:34 V29021MSA
0.951 µg/L 0.170 0.500Ethylbenzene 1 01/19/23 08:34 V29021MSA
141 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 01/21/23 18:22 V29073MSA
6.57 µg/L 0.470 1.00Naphthalene 1 01/19/23 08:34 V29021MSA
1.17 µg/L 0.220 0.500Toluene 1 01/19/23 08:34 V29021MSA
2.45 µg/L 0.210 0.500o-Xylene 1 01/19/23 08:34 V29021MSA
3.30 µg/L 0.420 1.00m,p-Xylene 1 01/19/23 08:34 V29021MSA
5.75 µg/L 0.210 0.500
Xylene (Total)1 01/19/23 08:34 V29021
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%01/19/23 08:341 MSA V29021
Surrogate: Dibromofluoromethane 97.4 Limits: 70-130%01/19/23 08:341 MSA V29021
Surrogate: 1,2-Dichloroethane - d4 94.6 Limits: 70-130%01/19/23 08:341 MSA V29021
Surrogate: Toluene-d8 98.2 Limits: 70-130%01/19/23 08:341 MSA V29021
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%01/21/23 18:2210 MSA V29073
Surrogate: Dibromofluoromethane 107 Limits: 70-130%01/21/23 18:2210 MSA V29073
Surrogate: 1,2-Dichloroethane - d4 93.8 Limits: 70-130%01/21/23 18:2210 MSA V29073
Surrogate: Toluene-d8 105 Limits: 70-130%01/21/23 18:2210 MSA V29073
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 6 of 14
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0102
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI # 5351 Received : 01/11/2023
Kingsway #10
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:RW-3
97295 Matrix:
1/9/2023 9:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00 V29072 01/21/23 09:00
1210 µg/L 18.0 50.0Benzene 100 01/21/23 20:52 V29073MSA
78.0 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 01/19/23 10:15 V29021MSA
527 µg/L 1.70 5.00Ethylbenzene 10 01/19/23 10:15 V29021MSA
105 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 01/19/23 10:15 V29021MSA
249 µg/L 4.70 10.0Naphthalene 10 01/19/23 10:15 V29021MSA
3260 µg/L 22.0 50.0Toluene 100 01/21/23 20:52 V29073MSA
864 µg/L 2.10 5.00o-Xylene 10 01/19/23 10:15 V29021MSA
1990 µg/L 4.20 10.0m,p-Xylene 10 01/19/23 10:15 V29021MSA
2850 µg/L 2.10 5.00
Xylene (Total)10 01/19/23 10:15 V29021
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%01/19/23 10:1510 MSA V29021
Surrogate: Dibromofluoromethane 95.6 Limits: 70-130%01/19/23 10:1510 MSA V29021
Surrogate: 1,2-Dichloroethane - d4 96.8 Limits: 70-130%01/19/23 10:1510 MSA V29021
Surrogate: Toluene-d8 105 Limits: 70-130%01/19/23 10:1510 MSA V29021
Surrogate: 4-Bromofluorobenzene 108 Limits: 70-130%01/21/23 20:52100 MSA V29073
Surrogate: Dibromofluoromethane 92.4 Limits: 70-130%01/21/23 20:52100 MSA V29073
Surrogate: 1,2-Dichloroethane - d4 97.6 Limits: 70-130%01/21/23 20:52100 MSA V29073
Surrogate: Toluene-d8 95.4 Limits: 70-130%01/21/23 20:52100 MSA V29073
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 14
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0102
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI # 5351 Received : 01/11/2023
Kingsway #10
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:Trip Blank
97296 Matrix:
1/9/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00
<0.180 µg/L 0.180 0.500Benzene 1 01/19/23 04:49 V29021MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 01/19/23 04:49 V29021MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 01/19/23 04:49 V29021MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 01/19/23 04:49 V29021MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 01/19/23 04:49 V29021MSA
<0.220 µg/L 0.220 0.500Toluene 1 01/19/23 04:49 V29021MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 01/19/23 04:49 V29021MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 01/19/23 04:49 V29021MSA
<0.21 µg/L 0.210 0.500
Xylene (Total)1 01/19/23 04:49 V29021
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%01/19/23 04:491 MSA V29021
Surrogate: Dibromofluoromethane 93.8 Limits: 70-130%01/19/23 04:491 MSA V29021
Surrogate: 1,2-Dichloroethane - d4 94.6 Limits: 70-130%01/19/23 04:491 MSA V29021
Surrogate: Toluene-d8 100 Limits: 70-130%01/19/23 04:491 MSA V29021
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 14
Quality Control Data
23-011-0102Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29021QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29020
Associated Lab Samples: 97293, 97294, 97295, 97296
LRB-V29020 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/19/23 03:580.5000.180<0.180µg/LBenzene
01/19/23 03:580.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
01/19/23 03:580.5000.170<0.170µg/LEthylbenzene
01/19/23 03:581.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
01/19/23 03:581.000.470<0.470µg/LNaphthalene
01/19/23 03:580.5000.220<0.220µg/LToluene
01/19/23 03:580.5000.210<0.210µg/Lo-Xylene
01/19/23 03:581.000.420<0.420µg/Lm,p-Xylene
01/19/23 03:584-Bromofluorobenzene (S)123 70-130
01/19/23 03:58Dibromofluoromethane (S)93.0 70-130
01/19/23 03:581,2-Dichloroethane - d4 (S)97.0 70-130
01/19/23 03:58Toluene-d8 (S)95.4 70-130
LCS-V29020 LCSD-V29020Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.3 96.599.019.820.0µg/LBenzene 70-130 2.5 20.0
19.2 96.010020.020.0µg/LDi-Isopropyl Ether (DIPE)70-130 4.0 20.0
19.3 96.510621.120.0µg/LEthylbenzene 70-130 8.9 20.0
18.6 93.094.518.920.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.6 20.0
19.8 99.010420.720.0µg/LNaphthalene 70-130 4.4 20.0
20.4 10298.019.620.0µg/LToluene 70-130 4.0 20.0
19.3 96.510521.020.0µg/Lo-Xylene 70-130 8.4 20.0
40.1 10010943.540.0µg/Lm,p-Xylene 70-130 8.1 20.0
98.61034-Bromofluorobenzene (S)70-130
98.096.2Dibromofluoromethane (S)70-130
Page 1 of 4Date:01/24/2023 03:52 PM
Page 9 of 14
Quality Control Data
23-011-0102Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29021QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29020
LCS-V29020 LCSD-V29020Laboratory Control Sample & LCSD
LCSD
ResultParameter
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
97.296.21,2-Dichloroethane - d4 (S)70-130
101104Toluene-d8 (S)70-130
Page 2 of 4Date:01/24/2023 03:52 PM
Page 10 of 14
Quality Control Data
23-011-0102Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29073QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29072
Associated Lab Samples: 97293, 97294, 97295
LRB-V29072 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/21/23 13:470.5000.180<0.180µg/LBenzene
01/21/23 13:470.5000.170<0.170µg/LEthylbenzene
01/21/23 13:471.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
01/21/23 13:471.000.470<0.470µg/LNaphthalene
01/21/23 13:470.5000.220<0.220µg/LToluene
01/21/23 13:470.5000.210<0.210µg/Lo-Xylene
01/21/23 13:471.000.420<0.420µg/Lm,p-Xylene
01/21/23 13:474-Bromofluorobenzene (S)97.2 70-130
01/21/23 13:47Dibromofluoromethane (S)104 70-130
01/21/23 13:471,2-Dichloroethane - d4 (S)104 70-130
01/21/23 13:47Toluene-d8 (S)94.2 70-130
LCS-V29072 LCSD-V29072Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.1 90.592.018.420.0µg/LBenzene 70-130 1.6 20.0
19.4 97.097.019.420.0µg/LEthylbenzene 70-130 0.0 20.0
18.0 90.098.019.620.0µg/LMethyl tert-butyl ether (MTBE)70-130 8.5 20.0
20.1 10111322.620.0µg/LNaphthalene 70-130 11.7 20.0
16.0 80.094.518.920.0µg/LToluene 70-130 16.6 20.0
18.0 90.089.517.920.0µg/Lo-Xylene 70-130 0.5 20.0
36.2 90.596.538.640.0µg/Lm,p-Xylene 70-130 6.4 20.0
96.41004-Bromofluorobenzene (S)70-130
96.4101Dibromofluoromethane (S)70-130
97.61001,2-Dichloroethane - d4 (S)70-130
Page 3 of 4Date:01/24/2023 03:52 PM
Page 11 of 14
Quality Control Data
23-011-0102Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29073QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29072
LCS-V29072 LCSD-V29072Laboratory Control Sample & LCSD
LCSD
ResultParameter
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
94.496.8Toluene-d8 (S)70-130
Page 4 of 4Date:01/24/2023 03:52 PM
Page 12 of 14
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-011-0102
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 2.3C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angela D Overcash Date & Time:01/11/2023 16:22:48
Special precautions or instructions included?
Comments:
Page 13 of 14
Page 14 of 14

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

3/8/2023
Geological Resources, Inc. Joanna Alley
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-055-0021 Client Project Description: Kingsway #10
GRI #5351
Dear Joanna Alley:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 2/24/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 140
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-055-0021
Page 2 of 140
Report Number:
Sample Summary Table
Client Project Description:
23-055-0021
Kingsway #10
GRI #5351
Lab No Client Sample ID Matrix Date Collected Date Received
02/23/2023 13:50Aqueous 89747 MW-3 02/24/2023
02/23/2023 13:31Aqueous 89748 MW-4 02/24/2023
02/23/2023 13:03Aqueous 89749 MW-5 02/24/2023
02/23/2023 13:12Aqueous 89750 MW-6 02/24/2023
02/23/2023 13:24Aqueous 89751 MW-7 02/24/2023
02/23/2023 12:52Aqueous 89752 MW-8 02/24/2023
02/23/2023 14:06Aqueous 89753 MW-9 02/24/2023
02/23/2023 12:31Aqueous 89754 MW-10 02/24/2023
02/23/2023 12:41Aqueous 89755 MW-11 02/24/2023
02/23/2023 12:20Aqueous 89756 MW-12 02/24/2023
02/23/2023 11:44Aqueous 89757 MW-13 02/24/2023
02/23/2023 11:18Aqueous 89758 MW-14 02/24/2023
02/23/2023 11:31Aqueous 89759 MW-15 02/24/2023
02/23/2023 11:06Aqueous 89760 MW-16 02/24/2023
02/23/2023 10:55Aqueous 89761 MW-17 02/24/2023
02/23/2023 10:44Aqueous 89762 MW-18 02/24/2023
02/23/2023 10:30Aqueous 89763 MW-19 02/24/2023
02/23/2023 15:03Aqueous 89764 TW-1 02/24/2023
02/23/2023 14:20Aqueous 89765 RW-1 02/24/2023
02/23/2023 14:33Aqueous 89766 RW-2 02/24/2023
02/23/2023 14:42Aqueous 89767 RW-3 02/24/2023
02/23/2023 09:15Aqueous 89768 Trip Blank 02/24/2023
Page 3 of 140
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-055-0021
Report Limit
Project:Kingsway #10
V 89747MW-3
2.36 02/28/2023 16:196200BChloroformµg/L 0.220
V 89748MW-4
J3.84 02/28/2023 16:446200BAcetoneµg/L 1.80
4.75 02/28/2023 16:446200BBromodichloromethaneµg/L 0.160
30.1 02/28/2023 16:446200BChloroformµg/L 0.220
V 89749MW-5
92.4 02/28/2023 21:126200BBenzeneµg/L 1.80
11.2 02/28/2023 21:126200BBromodichloromethaneµg/L 1.60
119 02/28/2023 21:126200BChloroformµg/L 2.20
139 02/28/2023 21:126200BDi-Isopropyl Ether (DIPE)µg/L 5.00
7.95 02/28/2023 21:126200B1,2-Dichlorobenzene µg/L 2.20
19.6 02/28/2023 21:126200B1,2-Dichloroethane µg/L 1.50
32.8 02/28/2023 21:126200BEthylbenzeneµg/L 1.70
J3.43 02/28/2023 21:126200BIsopropylbenzeneµg/L 1.80
J38.3 02/28/2023 21:126200BMethyl Ethyl Ketone (MEK)µg/L 7.10
669 02/28/2023 21:126200BMethyl tert-butyl ether (MTBE)µg/L 1.40
45.0 02/28/2023 21:126200B4-Methyl-2-Pentanone µg/L 0.780
J9.72 02/28/2023 21:126200BNaphthaleneµg/L 4.70
5.03 02/28/2023 21:126200Bn-Propylbenzene µg/L 1.90
822 02/28/2023 21:126200Btert-Butyl Alcohol (TBA)µg/L 16.0
1580 03/02/2023 02:236200Btert-Amyl Alcohol (TAA)µg/L 190
J19.6 02/28/2023 21:126200Btert-Amyl Methyl Ether (TAME)µg/L 2.80
18.7 02/28/2023 21:126200BTolueneµg/L 2.20
44.3 02/28/2023 21:126200B1,2,4-Trimethylbenzene µg/L 1.90
21.1 02/28/2023 21:126200B1,3,5-Trimethylbenzene µg/L 1.80
54.4 02/28/2023 21:126200Bo-Xylene µg/L 2.10
124 02/28/2023 21:126200Bm,p-Xylene µg/L 4.20
178 02/28/2023 21:126200BXylene (Total)µg/L 2.10
V 89750MW-6
1.14 02/28/2023 17:086200BDi-Isopropyl Ether (DIPE)µg/L 0.500
1.05 02/28/2023 17:086200BMethyl tert-butyl ether (MTBE)µg/L 0.140
V 89751MW-7
6.85 02/28/2023 17:336200BDi-Isopropyl Ether (DIPE)µg/L 0.500
3.11 02/28/2023 17:336200BMethyl tert-butyl ether (MTBE)µg/L 0.140
Page 4 of 140
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-055-0021
Report Limit
Project:Kingsway #10
V 89751MW-7
44.9 02/28/2023 17:336200Btert-Butyl Alcohol (TBA)µg/L 1.60
V 89752MW-8
0.941 02/28/2023 17:576200BBenzeneµg/L 0.180
2.46 02/28/2023 17:576200BChloroformµg/L 0.220
4.66 02/28/2023 17:576200BDi-Isopropyl Ether (DIPE)µg/L 0.500
0.697 02/28/2023 17:576200BEthylbenzeneµg/L 0.170
19.2 02/28/2023 17:576200BMethyl tert-butyl ether (MTBE)µg/L 0.140
J1.68 02/28/2023 17:576200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
2.58 02/28/2023 17:576200B1,2,4-Trimethylbenzene µg/L 0.190
2.92 02/28/2023 17:576200B1,3,5-Trimethylbenzene µg/L 0.180
4.50 02/28/2023 17:576200Bo-Xylene µg/L 0.210
7.21 02/28/2023 17:576200Bm,p-Xylene µg/L 0.420
11.7 02/28/2023 17:576200BXylene (Total)µg/L 0.210
V 89753MW-9
5230 03/02/2023 03:116200BBenzeneµg/L 90.0
23.6 02/28/2023 21:366200Bn-Butylbenzene µg/L 1.80
8.67 02/28/2023 21:366200Bsec-Butyl benzene µg/L 2.00
191 02/28/2023 21:366200BDi-Isopropyl Ether (DIPE)µg/L 5.00
101 02/28/2023 21:366200B1,2-Dibromoethane µg/L 2.00
35.5 02/28/2023 21:366200B1,2-Dichloroethane µg/L 1.50
1230 03/02/2023 03:116200BEthylbenzeneµg/L 85.0
47.2 02/28/2023 21:366200BIsopropylbenzeneµg/L 1.80
J4.56 02/28/2023 21:366200B4-Isopropyl toluene µg/L 0.890
158 02/28/2023 21:366200BMethyl tert-butyl ether (MTBE)µg/L 1.40
427 02/28/2023 21:366200BNaphthaleneµg/L 4.70
139 02/28/2023 21:366200Bn-Propylbenzene µg/L 1.90
81.5 02/28/2023 21:366200BStyreneµg/L 2.20
382 02/28/2023 21:366200Btert-Butyl Alcohol (TBA)µg/L 16.0
2050 03/02/2023 03:116200Btert-Amyl Alcohol (TAA)µg/L 950
9000 03/02/2023 03:116200BTolueneµg/L 110
905 03/02/2023 03:116200B1,2,4-Trimethylbenzene µg/L 95.0
293 02/28/2023 21:366200B1,3,5-Trimethylbenzene µg/L 1.80
1740 03/02/2023 03:116200Bo-Xylene µg/L 105
3790 03/02/2023 03:116200Bm,p-Xylene µg/L 210
5530 03/02/2023 03:116200BXylene (Total)µg/L 105
Page 5 of 140
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-055-0021
Report Limit
Project:Kingsway #10
V 89754MW-10
68.8 02/28/2023 19:106200BAcetoneµg/L 1.80
95.1 02/28/2023 19:106200BBenzeneµg/L 0.180
5.03 02/28/2023 19:106200BBromodichloromethaneµg/L 0.160
J0.474 02/28/2023 19:106200Bn-Butylbenzene µg/L 0.180
J0.373 02/28/2023 19:106200Bsec-Butyl benzene µg/L 0.200
5.42 02/28/2023 19:106200BChlorobenzeneµg/L 0.190
2.99 02/28/2023 19:106200BChlorodibromomethaneµg/L 0.190
43.7 02/28/2023 19:106200BChloroformµg/L 0.220
2.75 02/28/2023 19:106200B2-Chlorotoluene µg/L 0.200
1.65 02/28/2023 19:106200B4-Chlorotoluene µg/L 0.200
80.4 02/28/2023 19:106200BDi-Isopropyl Ether (DIPE)µg/L 0.500
1.77 02/28/2023 19:106200B1,2-Dichlorobenzene µg/L 0.220
5.77 02/28/2023 19:106200B1,4-Dichlorobenzene µg/L 0.210
13.3 02/28/2023 19:106200B1,2-Dichloroethane µg/L 0.150
1.63 02/28/2023 19:106200B1,2-Dichloropropane µg/L 0.190
19.7 02/28/2023 19:106200BEthylbenzeneµg/L 0.170
8.38 02/28/2023 19:106200B2-Hexanone µg/L 0.380
1.81 02/28/2023 19:106200BIsopropylbenzeneµg/L 0.180
J0.371 02/28/2023 19:106200B4-Isopropyl toluene µg/L 0.089
45.1 02/28/2023 19:106200BMethyl Ethyl Ketone (MEK)µg/L 0.710
207 03/02/2023 01:586200BMethyl tert-butyl ether (MTBE)µg/L 14.0
10.6 02/28/2023 19:106200B4-Methyl-2-Pentanone µg/L 0.078
2.70 02/28/2023 19:106200BMethylene Chloride µg/L 0.330
9.45 02/28/2023 19:106200BNaphthaleneµg/L 0.470
3.22 02/28/2023 19:106200Bn-Propylbenzene µg/L 0.190
199 02/28/2023 19:106200Btert-Butyl Alcohol (TBA)µg/L 1.60
1100 03/02/2023 01:586200Btert-Amyl Alcohol (TAA)µg/L 190
J7.84 02/28/2023 19:106200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
1.18 02/28/2023 19:106200B1,1,2,2-Tetrachloroethane µg/L 0.160
0.561 02/28/2023 19:106200BTetrachloroetheneµg/L 0.220
22.1 02/28/2023 19:106200BTolueneµg/L 0.220
J0.384 02/28/2023 19:106200BTrichloroetheneµg/L 0.180
46.0 02/28/2023 19:106200B1,2,4-Trimethylbenzene µg/L 0.190
3.94 02/28/2023 19:106200B1,3,5-Trimethylbenzene µg/L 0.180
66.3 02/28/2023 19:106200Bo-Xylene µg/L 0.210
146 02/28/2023 19:106200Bm,p-Xylene µg/L 0.420
212 02/28/2023 19:106200BXylene (Total)µg/L 0.210
Page 6 of 140
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-055-0021
Report Limit
Project:Kingsway #10
V 89755MW-11
19.0 02/28/2023 18:226200BBenzeneµg/L 0.180
0.648 02/28/2023 18:226200BEthylbenzeneµg/L 0.170
0.533 02/28/2023 18:226200BIsopropylbenzeneµg/L 0.180
1.32 02/28/2023 18:226200BNaphthaleneµg/L 0.470
0.533 02/28/2023 18:226200Bn-Propylbenzene µg/L 0.190
86.1 02/28/2023 18:226200Btert-Butyl Alcohol (TBA)µg/L 1.60
1.54 02/28/2023 18:226200Bo-Xylene µg/L 0.210
7.26 02/28/2023 18:226200Bm,p-Xylene µg/L 0.420
8.80 02/28/2023 18:226200BXylene (Total)µg/L 0.210
V 89756MW-12
0.658 02/28/2023 18:466200BBenzeneµg/L 0.180
1.55 02/28/2023 18:466200BChloroformµg/L 0.220
4.17 02/28/2023 18:466200BDi-Isopropyl Ether (DIPE)µg/L 0.500
0.597 02/28/2023 18:466200BEthylbenzeneµg/L 0.170
57.6 02/28/2023 18:466200BMethyl tert-butyl ether (MTBE)µg/L 0.140
1.15 02/28/2023 18:466200BNaphthaleneµg/L 0.470
55.3 02/28/2023 18:466200Btert-Butyl Alcohol (TBA)µg/L 1.60
J2.57 02/28/2023 18:466200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
0.761 02/28/2023 18:466200B1,2,4-Trimethylbenzene µg/L 0.190
2.15 02/28/2023 18:466200Bo-Xylene µg/L 0.210
3.85 02/28/2023 18:466200Bm,p-Xylene µg/L 0.420
6.00 02/28/2023 18:466200BXylene (Total)µg/L 0.210
V 89758MW-14
1.02 03/01/2023 02:546200BChloroformµg/L 0.220
1.53 03/01/2023 02:546200BDi-Isopropyl Ether (DIPE)µg/L 0.500
1.62 03/01/2023 02:546200BMethyl tert-butyl ether (MTBE)µg/L 0.140
V 89759MW-15
7610 03/01/2023 07:226200BBenzeneµg/L 18.0
884 03/01/2023 07:226200BDi-Isopropyl Ether (DIPE)µg/L 50.0
199 03/01/2023 07:226200B1,2-Dichloroethane µg/L 15.0
67600 03/01/2023 07:226200BEthanolµg/L 4200
985 03/01/2023 07:226200BEthylbenzeneµg/L 17.0
J36.4 03/01/2023 07:226200BIsopropylbenzeneµg/L 18.0
586 03/01/2023 07:226200BMethyl Ethyl Ketone (MEK)µg/L 71.0
1280 03/01/2023 07:226200BMethyl tert-butyl ether (MTBE)µg/L 14.0
Page 7 of 140
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-055-0021
Report Limit
Project:Kingsway #10
V 89759MW-15
422 03/01/2023 07:226200BNaphthaleneµg/L 47.0
104 03/01/2023 07:226200Bn-Propylbenzene µg/L 19.0
1350 03/01/2023 07:226200Btert-Butyl Alcohol (TBA)µg/L 160
4170 03/01/2023 07:226200Btert-Amyl Alcohol (TAA)µg/L 190
8480 03/07/2023 09:146200BTolueneµg/L 22.0
694 03/01/2023 07:226200B1,2,4-Trimethylbenzene µg/L 19.0
231 03/01/2023 07:226200B1,3,5-Trimethylbenzene µg/L 18.0
1320 03/01/2023 07:226200Bo-Xylene µg/L 21.0
3400 03/01/2023 07:226200Bm,p-Xylene µg/L 42.0
4720 03/01/2023 07:226200BXylene (Total)µg/L 21.0
V 89761MW-17
J2.92 03/01/2023 03:426200BAcetoneµg/L 1.80
1.07 03/01/2023 03:426200BNaphthaleneµg/L 0.470
2.21 03/01/2023 03:426200BTolueneµg/L 0.220
V 89762MW-18
2.77 03/01/2023 06:096200BNaphthaleneµg/L 0.470
V 89763MW-19
2.01 03/01/2023 04:076200BDi-Isopropyl Ether (DIPE)µg/L 0.500
V 89764TW-1
1.85 03/01/2023 04:316200BBenzeneµg/L 0.180
1.45 03/01/2023 04:316200BChloroformµg/L 0.220
6.74 03/01/2023 04:316200BDi-Isopropyl Ether (DIPE)µg/L 0.500
J0.303 03/01/2023 04:316200B1,2-Dichloroethane µg/L 0.150
J0.460 03/01/2023 04:316200BEthylbenzeneµg/L 0.170
1.24 03/01/2023 04:316200BNaphthaleneµg/L 0.470
135 03/01/2023 04:316200Btert-Butyl Alcohol (TBA)µg/L 1.60
41.2 03/01/2023 04:316200Btert-Amyl Alcohol (TAA)µg/L 1.90
0.501 03/01/2023 04:316200Bo-Xylene µg/L 0.210
0.501 03/01/2023 04:316200BXylene (Total)µg/L 0.210
V 89765RW-1
6800 03/01/2023 07:476200BBenzeneµg/L 18.0
J37.1 03/01/2023 07:476200Bn-Butylbenzene µg/L 18.0
191 03/01/2023 07:476200BDi-Isopropyl Ether (DIPE)µg/L 50.0
2380 03/01/2023 07:476200BEthylbenzeneµg/L 17.0
Page 8 of 140
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-055-0021
Report Limit
Project:Kingsway #10
V 89765RW-1
81.5 03/01/2023 07:476200BIsopropylbenzeneµg/L 18.0
929 03/01/2023 07:476200BNaphthaleneµg/L 47.0
252 03/01/2023 07:476200Bn-Propylbenzene µg/L 19.0
109 03/01/2023 07:476200BStyreneµg/L 22.0
1970 03/01/2023 07:476200Btert-Amyl Alcohol (TAA)µg/L 190
25400 03/01/2023 08:116200BTolueneµg/L 220
2220 03/01/2023 07:476200B1,2,4-Trimethylbenzene µg/L 19.0
634 03/01/2023 07:476200B1,3,5-Trimethylbenzene µg/L 18.0
4090 03/01/2023 07:476200Bo-Xylene µg/L 21.0
10300 03/01/2023 07:476200Bm,p-Xylene µg/L 42.0
14400 03/01/2023 07:476200BXylene (Total)µg/L 21.0
V 89766RW-2
6.51 03/01/2023 06:346200BBenzeneµg/L 0.180
0.769 03/01/2023 06:346200Bn-Butylbenzene µg/L 0.180
0.542 03/01/2023 06:346200Bsec-Butyl benzene µg/L 0.200
5.47 03/01/2023 06:346200BChloroformµg/L 0.220
14.0 03/01/2023 06:346200BDi-Isopropyl Ether (DIPE)µg/L 0.500
17.0 03/01/2023 06:346200BEthylbenzeneµg/L 0.170
9.86 03/01/2023 06:346200B2-Hexanone µg/L 0.380
1.24 03/01/2023 06:346200BIsopropylbenzeneµg/L 0.180
0.508 03/01/2023 06:346200B4-Isopropyl toluene µg/L 0.089
90.4 03/01/2023 06:346200BMethyl tert-butyl ether (MTBE)µg/L 0.140
12.1 03/01/2023 06:346200BNaphthaleneµg/L 0.470
2.76 03/01/2023 06:346200Bn-Propylbenzene µg/L 0.190
237 03/02/2023 01:346200Btert-Butyl Alcohol (TBA)µg/L 16.0
187 03/02/2023 01:346200Btert-Amyl Alcohol (TAA)µg/L 19.0
J3.55 03/01/2023 06:346200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
64.4 03/01/2023 06:346200BTolueneµg/L 0.220
59.1 03/01/2023 06:346200B1,2,4-Trimethylbenzene µg/L 0.190
19.1 03/01/2023 06:346200B1,3,5-Trimethylbenzene µg/L 0.180
67.4 03/01/2023 06:346200Bo-Xylene µg/L 0.210
169 03/01/2023 06:346200Bm,p-Xylene µg/L 0.420
236 03/01/2023 06:346200BXylene (Total)µg/L 0.210
V 89767RW-3
1030 03/02/2023 02:476200BBenzeneµg/L 18.0
4.61 03/01/2023 04:566200BBromomethaneµg/L 0.280
Page 9 of 140
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-055-0021
Report Limit
Project:Kingsway #10
V 89767RW-3
9.87 03/01/2023 04:566200Bn-Butylbenzene µg/L 0.180
4.37 03/01/2023 04:566200Bsec-Butyl benzene µg/L 0.200
63.9 03/01/2023 04:566200BDi-Isopropyl Ether (DIPE)µg/L 0.500
16.5 03/01/2023 04:566200B1,2-Dibromoethane µg/L 0.200
14.9 03/01/2023 04:566200B1,2-Dichloroethane µg/L 0.150
564 03/02/2023 02:476200BEthylbenzeneµg/L 17.0
31.5 03/01/2023 04:566200B2-Hexanone µg/L 0.380
28.9 03/01/2023 04:566200BIsopropylbenzeneµg/L 0.180
2.82 03/01/2023 04:566200B4-Isopropyl toluene µg/L 0.089
91.8 03/01/2023 04:566200BMethyl tert-butyl ether (MTBE)µg/L 0.140
211 03/02/2023 02:476200BNaphthaleneµg/L 47.0
86.0 03/01/2023 04:566200Bn-Propylbenzene µg/L 0.190
24.3 03/01/2023 04:566200BStyreneµg/L 0.220
J60803/02/2023 02:476200Btert-Butyl Alcohol (TBA)µg/L 160
635 03/02/2023 02:476200Btert-Amyl Alcohol (TAA)µg/L 190
3110 03/02/2023 02:476200BTolueneµg/L 22.0
621 03/02/2023 02:476200B1,2,4-Trimethylbenzene µg/L 19.0
155 03/02/2023 02:476200B1,3,5-Trimethylbenzene µg/L 18.0
797 03/02/2023 02:476200Bo-Xylene µg/L 21.0
1940 03/02/2023 02:476200Bm,p-Xylene µg/L 42.0
2740 03/02/2023 02:476200BXylene (Total)µg/L 21.0
Page 10 of 140

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Kingsway #10 Lab Report Number: 23-055-0021
Date: 3/8/2023
Volatile Organic Compounds - GC/MS Method 6200B Analyte: 3,3-Dimethyl-1-butanol QC Batch No: V30280/V30279
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: 4-Methyl-2-pentanone QC Batch No: V30378/V30279
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: Bromoform QC Batch No: V30280/V30279
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: Bromoform QC Batch No: V30378/V30279
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: 1,2-Dibromo-3-chloropropane QC Batch No: V30378/V30279
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable. Analyte: Ethanol QC Batch No: V30280/V30279
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: tert-Butyl alcohol QC Batch No: V30378/V30279 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Analyte: Vinyl acetate QC Batch No: V30280/V30279
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Page 11 of 140

Analyte: Vinyl acetate
QC Batch No: V30378/V30279 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.

Page 12 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-3
89747 Matrix:
2/23/2023 13:50
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 02/28/23 16:19 6200BMSA
Surrogate: 4-Bromofluorobenzene 93.2 Limits: 70-130%02/28/23 16:191 MSA V30280
Surrogate: Dibromofluoromethane 101 Limits: 70-130%02/28/23 16:191 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%02/28/23 16:191 MSA V30280
Surrogate: Toluene-d8 103 Limits: 70-130%02/28/23 16:191 MSA V30280
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-3
89747 Matrix:
2/23/2023 13:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 02/28/23 16:19 V30280MSA
<0.180 µg/L 0.180 0.500Benzene 1 02/28/23 16:19 V30280MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/28/23 16:19 V30280MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/28/23 16:19 V30280MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/28/23 16:19 V30280MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/28/23 16:19 V30280MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/28/23 16:19 V30280MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 02/28/23 16:19 V30280MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 02/28/23 16:19 V30280MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/28/23 16:19 V30280MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/28/23 16:19 V30280MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/28/23 16:19 V30280MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/28/23 16:19 V30280MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/28/23 16:19 V30280MSA
2.36 µg/L 0.220 0.500Chloroform 1 02/28/23 16:19 V30280MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 02/28/23 16:19 V30280MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/28/23 16:19 V30280MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/28/23 16:19 V30280MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 02/28/23 16:19 V30280MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/28/23 16:19 V30280MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/28/23 16:19 V30280MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/28/23 16:19 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-3
89747 Matrix:
2/23/2023 13:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/28/23 16:19 V30280MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/28/23 16:19 V30280MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/28/23 16:19 V30280MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/28/23 16:19 V30280MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/28/23 16:19 V30280MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/28/23 16:19 V30280MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/28/23 16:19 V30280MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/28/23 16:19 V30280MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 02/28/23 16:19 V30280MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/28/23 16:19 V30280MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/28/23 16:19 V30280MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/28/23 16:19 V30280MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/28/23 16:19 V30280MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/28/23 16:19 V30280MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/28/23 16:19 V30280MSA
<42.0 µg/L 42.0 200
Ethanol 1 02/28/23 16:19 V30280MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 02/28/23 16:19 V30280MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 02/28/23 16:19 V30280MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 02/28/23 16:19 V30280MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 02/28/23 16:19 V30280MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/28/23 16:19 V30280MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/28/23 16:19 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-3
89747 Matrix:
2/23/2023 13:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 02/28/23 16:19 V30280MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 02/28/23 16:19 V30280MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 02/28/23 16:19 V30280MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 02/28/23 16:19 V30280MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 02/28/23 16:19 V30280MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/28/23 16:19 V30280MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 02/28/23 16:19 V30280MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 02/28/23 16:19 V30280MSA
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 02/28/23 16:19 V30280MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 02/28/23 16:19 V30280MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/28/23 16:19 V30280MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/28/23 16:19 V30280MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/28/23 16:19 V30280MSA
<0.220 µg/L 0.220 0.500Toluene 1 02/28/23 16:19 V30280MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 02/28/23 16:19 V30280MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 02/28/23 16:19 V30280MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/28/23 16:19 V30280MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/28/23 16:19 V30280MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/28/23 16:19 V30280MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/28/23 16:19 V30280MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 02/28/23 16:19 V30280MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 02/28/23 16:19 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-3
89747 Matrix:
2/23/2023 13:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/28/23 16:19 V30280MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 02/28/23 16:19 V30280MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/28/23 16:19 V30280MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 02/28/23 16:19 V30280MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 02/28/23 16:19 V30280MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 02/28/23 16:19 V30280
Surrogate: 4-Bromofluorobenzene 93.2 Limits: 70-130%02/28/23 16:191 MSA V30280
Surrogate: Dibromofluoromethane 101 Limits: 70-130%02/28/23 16:191 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%02/28/23 16:191 MSA V30280
Surrogate: Toluene-d8 103 Limits: 70-130%02/28/23 16:191 MSA V30280
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-4
89748 Matrix:
2/23/2023 13:31
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 02/28/23 16:44 6200BMSA
Surrogate: 4-Bromofluorobenzene 94.4 Limits: 70-130%02/28/23 16:441 MSA V30280
Surrogate: Dibromofluoromethane 97.0 Limits: 70-130%02/28/23 16:441 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 108 Limits: 70-130%02/28/23 16:441 MSA V30280
Surrogate: Toluene-d8 106 Limits: 70-130%02/28/23 16:441 MSA V30280
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-4
89748 Matrix:
2/23/2023 13:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
3.84 J µg/L 1.80 10.0Acetone 1 02/28/23 16:44 V30280MSA
<0.180 µg/L 0.180 0.500Benzene 1 02/28/23 16:44 V30280MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/28/23 16:44 V30280MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/28/23 16:44 V30280MSA
4.75 µg/L 0.160 0.500Bromodichloromethane 1 02/28/23 16:44 V30280MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/28/23 16:44 V30280MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/28/23 16:44 V30280MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 02/28/23 16:44 V30280MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 02/28/23 16:44 V30280MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/28/23 16:44 V30280MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/28/23 16:44 V30280MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/28/23 16:44 V30280MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/28/23 16:44 V30280MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/28/23 16:44 V30280MSA
30.1 µg/L 0.220 0.500Chloroform 1 02/28/23 16:44 V30280MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 02/28/23 16:44 V30280MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/28/23 16:44 V30280MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/28/23 16:44 V30280MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 02/28/23 16:44 V30280MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/28/23 16:44 V30280MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/28/23 16:44 V30280MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/28/23 16:44 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-4
89748 Matrix:
2/23/2023 13:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/28/23 16:44 V30280MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/28/23 16:44 V30280MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/28/23 16:44 V30280MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/28/23 16:44 V30280MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/28/23 16:44 V30280MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/28/23 16:44 V30280MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/28/23 16:44 V30280MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/28/23 16:44 V30280MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 02/28/23 16:44 V30280MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/28/23 16:44 V30280MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/28/23 16:44 V30280MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/28/23 16:44 V30280MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/28/23 16:44 V30280MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/28/23 16:44 V30280MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/28/23 16:44 V30280MSA
<42.0 µg/L 42.0 200
Ethanol 1 02/28/23 16:44 V30280MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 02/28/23 16:44 V30280MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 02/28/23 16:44 V30280MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 02/28/23 16:44 V30280MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 02/28/23 16:44 V30280MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/28/23 16:44 V30280MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/28/23 16:44 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-4
89748 Matrix:
2/23/2023 13:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 02/28/23 16:44 V30280MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 02/28/23 16:44 V30280MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 02/28/23 16:44 V30280MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 02/28/23 16:44 V30280MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 02/28/23 16:44 V30280MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/28/23 16:44 V30280MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 02/28/23 16:44 V30280MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 02/28/23 16:44 V30280MSA
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 02/28/23 16:44 V30280MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 02/28/23 16:44 V30280MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/28/23 16:44 V30280MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/28/23 16:44 V30280MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/28/23 16:44 V30280MSA
<0.220 µg/L 0.220 0.500Toluene 1 02/28/23 16:44 V30280MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 02/28/23 16:44 V30280MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 02/28/23 16:44 V30280MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/28/23 16:44 V30280MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/28/23 16:44 V30280MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/28/23 16:44 V30280MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/28/23 16:44 V30280MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 02/28/23 16:44 V30280MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 02/28/23 16:44 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-4
89748 Matrix:
2/23/2023 13:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/28/23 16:44 V30280MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 02/28/23 16:44 V30280MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/28/23 16:44 V30280MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 02/28/23 16:44 V30280MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 02/28/23 16:44 V30280MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 02/28/23 16:44 V30280
Surrogate: 4-Bromofluorobenzene 94.4 Limits: 70-130%02/28/23 16:441 MSA V30280
Surrogate: Dibromofluoromethane 97.0 Limits: 70-130%02/28/23 16:441 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 108 Limits: 70-130%02/28/23 16:441 MSA V30280
Surrogate: Toluene-d8 106 Limits: 70-130%02/28/23 16:441 MSA V30280
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-5
89749 Matrix:
2/23/2023 13:03
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 02/28/23 21:12 6200BMSA
Surrogate: 4-Bromofluorobenzene 96.2 Limits: 70-130%02/28/23 21:1210 MSA V30280
Surrogate: Dibromofluoromethane 95.8 Limits: 70-130%02/28/23 21:1210 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 108 Limits: 70-130%02/28/23 21:1210 MSA V30280
Surrogate: Toluene-d8 106 Limits: 70-130%02/28/23 21:1210 MSA V30280
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%03/02/23 02:23100 MSA V30431
Surrogate: Dibromofluoromethane 98.8 Limits: 70-130%03/02/23 02:23100 MSA V30431
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%03/02/23 02:23100 MSA V30431
Surrogate: Toluene-d8 100 Limits: 70-130%03/02/23 02:23100 MSA V30431
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-5
89749 Matrix:
2/23/2023 13:03
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00 V30429 03/01/23 09:00
<18.0 µg/L 18.0 100Acetone 10 02/28/23 21:12 V30280MSA
92.4 µg/L 1.80 5.00Benzene 10 02/28/23 21:12 V30280MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 02/28/23 21:12 V30280MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 02/28/23 21:12 V30280MSA
11.2 µg/L 1.60 5.00Bromodichloromethane 10 02/28/23 21:12 V30280MSA
<15.0 µg/L 15.0 50.0Bromoform 10 02/28/23 21:12 V30280MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 02/28/23 21:12 V30280MSA
<1.80 µg/L 1.80 5.00n-Butylbenzene 10 02/28/23 21:12 V30280MSA
<2.00 µg/L 2.00 5.00
sec-Butyl benzene 10 02/28/23 21:12 V30280MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 02/28/23 21:12 V30280MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 02/28/23 21:12 V30280MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 02/28/23 21:12 V30280MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 02/28/23 21:12 V30280MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 02/28/23 21:12 V30280MSA
119 µg/L 2.20 5.00Chloroform 10 02/28/23 21:12 V30280MSA
<2.20 µg/L 2.20 5.00
Chloromethane 10 02/28/23 21:12 V30280MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 02/28/23 21:12 V30280MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 02/28/23 21:12 V30280MSA
139 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 02/28/23 21:12 V30280MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 02/28/23 21:12 V30280MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 02/28/23 21:12 V30280MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 02/28/23 21:12 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-5
89749 Matrix:
2/23/2023 13:03
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00 V30429 03/01/23 09:00
7.95 µg/L 2.20 5.001,2-Dichlorobenzene 10 02/28/23 21:12 V30280MSA
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 02/28/23 21:12 V30280MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 02/28/23 21:12 V30280MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 02/28/23 21:12 V30280MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 02/28/23 21:12 V30280MSA
19.6 µg/L 1.50 5.001,2-Dichloroethane 10 02/28/23 21:12 V30280MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 02/28/23 21:12 V30280MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 02/28/23 21:12 V30280MSA
<1.80 µg/L 1.80 5.00
trans-1,2-Dichloroethene 10 02/28/23 21:12 V30280MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 02/28/23 21:12 V30280MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 02/28/23 21:12 V30280MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 02/28/23 21:12 V30280MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 02/28/23 21:12 V30280MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 02/28/23 21:12 V30280MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 02/28/23 21:12 V30280MSA
<420 µg/L 420 2000
Ethanol 10 02/28/23 21:12 V30280MSA
32.8 µg/L 1.70 5.00Ethylbenzene 10 02/28/23 21:12 V30280MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 02/28/23 21:12 V30280MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 02/28/23 21:12 V30280MSA
3.43 J µg/L 1.80 5.00Isopropylbenzene 10 02/28/23 21:12 V30280MSA
<0.890 µg/L 0.890 5.004-Isopropyl toluene 10 02/28/23 21:12 V30280MSA
38.3 J µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 02/28/23 21:12 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-5
89749 Matrix:
2/23/2023 13:03
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00 V30429 03/01/23 09:00
669 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 02/28/23 21:12 V30280MSA
45.0 µg/L 0.780 10.04-Methyl-2-Pentanone 10 02/28/23 21:12 V30280MSA
<3.30 µg/L 3.30 20.0Methylene Chloride 10 02/28/23 21:12 V30280MSA
9.72 J µg/L 4.70 10.0Naphthalene 10 02/28/23 21:12 V30280MSA
5.03 µg/L 1.90 5.00n-Propylbenzene 10 02/28/23 21:12 V30280MSA
<2.20 µg/L 2.20 5.00Styrene 10 02/28/23 21:12 V30280MSA
822 µg/L 16.0 100tert-Butyl Alcohol (TBA)10 02/28/23 21:12 V30280MSA
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 02/28/23 21:12 V30280MSA
1580 µg/L 190 1000
tert-Amyl Alcohol (TAA)100 03/02/23 02:23 V30431MSA
19.6 J µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 02/28/23 21:12 V30280MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 02/28/23 21:12 V30280MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 02/28/23 21:12 V30280MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 02/28/23 21:12 V30280MSA
18.7 µg/L 2.20 5.00Toluene 10 02/28/23 21:12 V30280MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 02/28/23 21:12 V30280MSA
<3.10 µg/L 3.10 5.00
1,2,4-Trichlorobenzene 10 02/28/23 21:12 V30280MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 02/28/23 21:12 V30280MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 02/28/23 21:12 V30280MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 02/28/23 21:12 V30280MSA
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 02/28/23 21:12 V30280MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 02/28/23 21:12 V30280MSA
44.3 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 02/28/23 21:12 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-5
89749 Matrix:
2/23/2023 13:03
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00 V30429 03/01/23 09:00
21.1 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 02/28/23 21:12 V30280MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 02/28/23 21:12 V30280MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 02/28/23 21:12 V30280MSA
54.4 µg/L 2.10 5.00o-Xylene 10 02/28/23 21:12 V30280MSA
124 µg/L 4.20 10.0m,p-Xylene 10 02/28/23 21:12 V30280MSA
178 µg/L 2.10 5.00Xylene (Total)10 02/28/23 21:12 V30280
Surrogate: 4-Bromofluorobenzene 96.2 Limits: 70-130%02/28/23 21:1210 MSA V30280
Surrogate: Dibromofluoromethane 95.8 Limits: 70-130%02/28/23 21:1210 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 108 Limits: 70-130%02/28/23 21:1210 MSA V30280
Surrogate: Toluene-d8 106 Limits: 70-130%02/28/23 21:1210 MSA V30280
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%03/02/23 02:23100 MSA V30431
Surrogate: Dibromofluoromethane 98.8 Limits: 70-130%03/02/23 02:23100 MSA V30431
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%03/02/23 02:23100 MSA V30431
Surrogate: Toluene-d8 100 Limits: 70-130%03/02/23 02:23100 MSA V30431
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-6
89750 Matrix:
2/23/2023 13:12
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 02/28/23 17:08 6200BMSA
Surrogate: 4-Bromofluorobenzene 94.4 Limits: 70-130%02/28/23 17:081 MSA V30280
Surrogate: Dibromofluoromethane 98.2 Limits: 70-130%02/28/23 17:081 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%02/28/23 17:081 MSA V30280
Surrogate: Toluene-d8 107 Limits: 70-130%02/28/23 17:081 MSA V30280
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-6
89750 Matrix:
2/23/2023 13:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 02/28/23 17:08 V30280MSA
<0.180 µg/L 0.180 0.500Benzene 1 02/28/23 17:08 V30280MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/28/23 17:08 V30280MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/28/23 17:08 V30280MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/28/23 17:08 V30280MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/28/23 17:08 V30280MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/28/23 17:08 V30280MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 02/28/23 17:08 V30280MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 02/28/23 17:08 V30280MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/28/23 17:08 V30280MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/28/23 17:08 V30280MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/28/23 17:08 V30280MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/28/23 17:08 V30280MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/28/23 17:08 V30280MSA
<0.220 µg/L 0.220 0.500Chloroform 1 02/28/23 17:08 V30280MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 02/28/23 17:08 V30280MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/28/23 17:08 V30280MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/28/23 17:08 V30280MSA
1.14 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 02/28/23 17:08 V30280MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/28/23 17:08 V30280MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/28/23 17:08 V30280MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/28/23 17:08 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-6
89750 Matrix:
2/23/2023 13:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/28/23 17:08 V30280MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/28/23 17:08 V30280MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/28/23 17:08 V30280MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/28/23 17:08 V30280MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/28/23 17:08 V30280MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/28/23 17:08 V30280MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/28/23 17:08 V30280MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/28/23 17:08 V30280MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 02/28/23 17:08 V30280MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/28/23 17:08 V30280MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/28/23 17:08 V30280MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/28/23 17:08 V30280MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/28/23 17:08 V30280MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/28/23 17:08 V30280MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/28/23 17:08 V30280MSA
<42.0 µg/L 42.0 200
Ethanol 1 02/28/23 17:08 V30280MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 02/28/23 17:08 V30280MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 02/28/23 17:08 V30280MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 02/28/23 17:08 V30280MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 02/28/23 17:08 V30280MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/28/23 17:08 V30280MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/28/23 17:08 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-6
89750 Matrix:
2/23/2023 13:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
1.05 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 02/28/23 17:08 V30280MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 02/28/23 17:08 V30280MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 02/28/23 17:08 V30280MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 02/28/23 17:08 V30280MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 02/28/23 17:08 V30280MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/28/23 17:08 V30280MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 02/28/23 17:08 V30280MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 02/28/23 17:08 V30280MSA
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 02/28/23 17:08 V30280MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 02/28/23 17:08 V30280MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/28/23 17:08 V30280MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/28/23 17:08 V30280MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/28/23 17:08 V30280MSA
<0.220 µg/L 0.220 0.500Toluene 1 02/28/23 17:08 V30280MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 02/28/23 17:08 V30280MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 02/28/23 17:08 V30280MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/28/23 17:08 V30280MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/28/23 17:08 V30280MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/28/23 17:08 V30280MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/28/23 17:08 V30280MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 02/28/23 17:08 V30280MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 02/28/23 17:08 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-6
89750 Matrix:
2/23/2023 13:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/28/23 17:08 V30280MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 02/28/23 17:08 V30280MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/28/23 17:08 V30280MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 02/28/23 17:08 V30280MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 02/28/23 17:08 V30280MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 02/28/23 17:08 V30280
Surrogate: 4-Bromofluorobenzene 94.4 Limits: 70-130%02/28/23 17:081 MSA V30280
Surrogate: Dibromofluoromethane 98.2 Limits: 70-130%02/28/23 17:081 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%02/28/23 17:081 MSA V30280
Surrogate: Toluene-d8 107 Limits: 70-130%02/28/23 17:081 MSA V30280
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-7
89751 Matrix:
2/23/2023 13:24
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 02/28/23 17:33 6200BMSA
Surrogate: 4-Bromofluorobenzene 95.2 Limits: 70-130%02/28/23 17:331 MSA V30280
Surrogate: Dibromofluoromethane 96.0 Limits: 70-130%02/28/23 17:331 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%02/28/23 17:331 MSA V30280
Surrogate: Toluene-d8 110 Limits: 70-130%02/28/23 17:331 MSA V30280
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-7
89751 Matrix:
2/23/2023 13:24
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 02/28/23 17:33 V30280MSA
<0.180 µg/L 0.180 0.500Benzene 1 02/28/23 17:33 V30280MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/28/23 17:33 V30280MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/28/23 17:33 V30280MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/28/23 17:33 V30280MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/28/23 17:33 V30280MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/28/23 17:33 V30280MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 02/28/23 17:33 V30280MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 02/28/23 17:33 V30280MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/28/23 17:33 V30280MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/28/23 17:33 V30280MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/28/23 17:33 V30280MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/28/23 17:33 V30280MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/28/23 17:33 V30280MSA
<0.220 µg/L 0.220 0.500Chloroform 1 02/28/23 17:33 V30280MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 02/28/23 17:33 V30280MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/28/23 17:33 V30280MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/28/23 17:33 V30280MSA
6.85 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 02/28/23 17:33 V30280MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/28/23 17:33 V30280MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/28/23 17:33 V30280MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/28/23 17:33 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-7
89751 Matrix:
2/23/2023 13:24
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/28/23 17:33 V30280MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/28/23 17:33 V30280MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/28/23 17:33 V30280MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/28/23 17:33 V30280MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/28/23 17:33 V30280MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/28/23 17:33 V30280MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/28/23 17:33 V30280MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/28/23 17:33 V30280MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 02/28/23 17:33 V30280MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/28/23 17:33 V30280MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/28/23 17:33 V30280MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/28/23 17:33 V30280MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/28/23 17:33 V30280MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/28/23 17:33 V30280MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/28/23 17:33 V30280MSA
<42.0 µg/L 42.0 200
Ethanol 1 02/28/23 17:33 V30280MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 02/28/23 17:33 V30280MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 02/28/23 17:33 V30280MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 02/28/23 17:33 V30280MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 02/28/23 17:33 V30280MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/28/23 17:33 V30280MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/28/23 17:33 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-7
89751 Matrix:
2/23/2023 13:24
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
3.11 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 02/28/23 17:33 V30280MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 02/28/23 17:33 V30280MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 02/28/23 17:33 V30280MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 02/28/23 17:33 V30280MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 02/28/23 17:33 V30280MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/28/23 17:33 V30280MSA
44.9 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 02/28/23 17:33 V30280MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 02/28/23 17:33 V30280MSA
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 02/28/23 17:33 V30280MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 02/28/23 17:33 V30280MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/28/23 17:33 V30280MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/28/23 17:33 V30280MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/28/23 17:33 V30280MSA
<0.220 µg/L 0.220 0.500Toluene 1 02/28/23 17:33 V30280MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 02/28/23 17:33 V30280MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 02/28/23 17:33 V30280MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/28/23 17:33 V30280MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/28/23 17:33 V30280MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/28/23 17:33 V30280MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/28/23 17:33 V30280MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 02/28/23 17:33 V30280MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 02/28/23 17:33 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-7
89751 Matrix:
2/23/2023 13:24
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/28/23 17:33 V30280MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 02/28/23 17:33 V30280MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/28/23 17:33 V30280MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 02/28/23 17:33 V30280MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 02/28/23 17:33 V30280MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 02/28/23 17:33 V30280
Surrogate: 4-Bromofluorobenzene 95.2 Limits: 70-130%02/28/23 17:331 MSA V30280
Surrogate: Dibromofluoromethane 96.0 Limits: 70-130%02/28/23 17:331 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%02/28/23 17:331 MSA V30280
Surrogate: Toluene-d8 110 Limits: 70-130%02/28/23 17:331 MSA V30280
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-8
89752 Matrix:
2/23/2023 12:52
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 02/28/23 17:57 6200BMSA
Surrogate: 4-Bromofluorobenzene 91.0 Limits: 70-130%02/28/23 17:571 MSA V30280
Surrogate: Dibromofluoromethane 101 Limits: 70-130%02/28/23 17:571 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 109 Limits: 70-130%02/28/23 17:571 MSA V30280
Surrogate: Toluene-d8 105 Limits: 70-130%02/28/23 17:571 MSA V30280
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-8
89752 Matrix:
2/23/2023 12:52
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 02/28/23 17:57 V30280MSA
0.941 µg/L 0.180 0.500Benzene 1 02/28/23 17:57 V30280MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/28/23 17:57 V30280MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/28/23 17:57 V30280MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/28/23 17:57 V30280MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/28/23 17:57 V30280MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/28/23 17:57 V30280MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 02/28/23 17:57 V30280MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 02/28/23 17:57 V30280MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/28/23 17:57 V30280MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/28/23 17:57 V30280MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/28/23 17:57 V30280MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/28/23 17:57 V30280MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/28/23 17:57 V30280MSA
2.46 µg/L 0.220 0.500Chloroform 1 02/28/23 17:57 V30280MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 02/28/23 17:57 V30280MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/28/23 17:57 V30280MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/28/23 17:57 V30280MSA
4.66 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 02/28/23 17:57 V30280MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/28/23 17:57 V30280MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/28/23 17:57 V30280MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/28/23 17:57 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-8
89752 Matrix:
2/23/2023 12:52
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/28/23 17:57 V30280MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/28/23 17:57 V30280MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/28/23 17:57 V30280MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/28/23 17:57 V30280MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/28/23 17:57 V30280MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/28/23 17:57 V30280MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/28/23 17:57 V30280MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/28/23 17:57 V30280MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 02/28/23 17:57 V30280MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/28/23 17:57 V30280MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/28/23 17:57 V30280MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/28/23 17:57 V30280MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/28/23 17:57 V30280MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/28/23 17:57 V30280MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/28/23 17:57 V30280MSA
<42.0 µg/L 42.0 200
Ethanol 1 02/28/23 17:57 V30280MSA
0.697 µg/L 0.170 0.500Ethylbenzene 1 02/28/23 17:57 V30280MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 02/28/23 17:57 V30280MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 02/28/23 17:57 V30280MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 02/28/23 17:57 V30280MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/28/23 17:57 V30280MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/28/23 17:57 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-8
89752 Matrix:
2/23/2023 12:52
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
19.2 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 02/28/23 17:57 V30280MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 02/28/23 17:57 V30280MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 02/28/23 17:57 V30280MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 02/28/23 17:57 V30280MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 02/28/23 17:57 V30280MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/28/23 17:57 V30280MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 02/28/23 17:57 V30280MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 02/28/23 17:57 V30280MSA
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 02/28/23 17:57 V30280MSA
1.68 J µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 02/28/23 17:57 V30280MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/28/23 17:57 V30280MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/28/23 17:57 V30280MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/28/23 17:57 V30280MSA
<0.220 µg/L 0.220 0.500Toluene 1 02/28/23 17:57 V30280MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 02/28/23 17:57 V30280MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 02/28/23 17:57 V30280MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/28/23 17:57 V30280MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/28/23 17:57 V30280MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/28/23 17:57 V30280MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/28/23 17:57 V30280MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 02/28/23 17:57 V30280MSA
2.58 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 02/28/23 17:57 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-8
89752 Matrix:
2/23/2023 12:52
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
2.92 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/28/23 17:57 V30280MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 02/28/23 17:57 V30280MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/28/23 17:57 V30280MSA
4.50 µg/L 0.210 0.500o-Xylene 1 02/28/23 17:57 V30280MSA
7.21 µg/L 0.420 1.00m,p-Xylene 1 02/28/23 17:57 V30280MSA
11.7 µg/L 0.210 0.500Xylene (Total)1 02/28/23 17:57 V30280
Surrogate: 4-Bromofluorobenzene 91.0 Limits: 70-130%02/28/23 17:571 MSA V30280
Surrogate: Dibromofluoromethane 101 Limits: 70-130%02/28/23 17:571 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 109 Limits: 70-130%02/28/23 17:571 MSA V30280
Surrogate: Toluene-d8 105 Limits: 70-130%02/28/23 17:571 MSA V30280
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-9
89753 Matrix:
2/23/2023 14:06
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 02/28/23 21:36 6200BMSA
Surrogate: 4-Bromofluorobenzene 95.8 Limits: 70-130%02/28/23 21:3610 MSA V30280
Surrogate: Dibromofluoromethane 84.2 Limits: 70-130%02/28/23 21:3610 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 120 Limits: 70-130%02/28/23 21:3610 MSA V30280
Surrogate: Toluene-d8 98.6 Limits: 70-130%02/28/23 21:3610 MSA V30280
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%03/02/23 03:11500 MSA V30431
Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%03/02/23 03:11500 MSA V30431
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%03/02/23 03:11500 MSA V30431
Surrogate: Toluene-d8 99.6 Limits: 70-130%03/02/23 03:11500 MSA V30431
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-9
89753 Matrix:
2/23/2023 14:06
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00 V30429 03/01/23 09:00
<18.0 µg/L 18.0 100Acetone 10 02/28/23 21:36 V30280MSA
5230 µg/L 90.0 250Benzene 500 03/02/23 03:11 V30431MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 02/28/23 21:36 V30280MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 02/28/23 21:36 V30280MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 02/28/23 21:36 V30280MSA
<15.0 µg/L 15.0 50.0Bromoform 10 02/28/23 21:36 V30280MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 02/28/23 21:36 V30280MSA
23.6 µg/L 1.80 5.00n-Butylbenzene 10 02/28/23 21:36 V30280MSA
8.67 µg/L 2.00 5.00
sec-Butyl benzene 10 02/28/23 21:36 V30280MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 02/28/23 21:36 V30280MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 02/28/23 21:36 V30280MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 02/28/23 21:36 V30280MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 02/28/23 21:36 V30280MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 02/28/23 21:36 V30280MSA
<2.20 µg/L 2.20 5.00Chloroform 10 02/28/23 21:36 V30280MSA
<2.20 µg/L 2.20 5.00
Chloromethane 10 02/28/23 21:36 V30280MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 02/28/23 21:36 V30280MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 02/28/23 21:36 V30280MSA
191 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 02/28/23 21:36 V30280MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 02/28/23 21:36 V30280MSA
101 µg/L 2.00 5.001,2-Dibromoethane 10 02/28/23 21:36 V30280MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 02/28/23 21:36 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-9
89753 Matrix:
2/23/2023 14:06
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00 V30429 03/01/23 09:00
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 02/28/23 21:36 V30280MSA
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 02/28/23 21:36 V30280MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 02/28/23 21:36 V30280MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 02/28/23 21:36 V30280MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 02/28/23 21:36 V30280MSA
35.5 µg/L 1.50 5.001,2-Dichloroethane 10 02/28/23 21:36 V30280MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 02/28/23 21:36 V30280MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 02/28/23 21:36 V30280MSA
<1.80 µg/L 1.80 5.00
trans-1,2-Dichloroethene 10 02/28/23 21:36 V30280MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 02/28/23 21:36 V30280MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 02/28/23 21:36 V30280MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 02/28/23 21:36 V30280MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 02/28/23 21:36 V30280MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 02/28/23 21:36 V30280MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 02/28/23 21:36 V30280MSA
<420 µg/L 420 2000
Ethanol 10 02/28/23 21:36 V30280MSA
1230 µg/L 85.0 250Ethylbenzene 500 03/02/23 03:11 V30431MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 02/28/23 21:36 V30280MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 02/28/23 21:36 V30280MSA
47.2 µg/L 1.80 5.00Isopropylbenzene 10 02/28/23 21:36 V30280MSA
4.56 J µg/L 0.890 5.004-Isopropyl toluene 10 02/28/23 21:36 V30280MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 02/28/23 21:36 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-9
89753 Matrix:
2/23/2023 14:06
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00 V30429 03/01/23 09:00
158 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 02/28/23 21:36 V30280MSA
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 02/28/23 21:36 V30280MSA
<3.30 µg/L 3.30 20.0Methylene Chloride 10 02/28/23 21:36 V30280MSA
427 µg/L 4.70 10.0Naphthalene 10 02/28/23 21:36 V30280MSA
139 µg/L 1.90 5.00n-Propylbenzene 10 02/28/23 21:36 V30280MSA
81.5 µg/L 2.20 5.00Styrene 10 02/28/23 21:36 V30280MSA
382 µg/L 16.0 100tert-Butyl Alcohol (TBA)10 02/28/23 21:36 V30280MSA
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 02/28/23 21:36 V30280MSA
2050 µg/L 950 5000
tert-Amyl Alcohol (TAA)500 03/02/23 03:11 V30431MSA
<2.80 µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 02/28/23 21:36 V30280MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 02/28/23 21:36 V30280MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 02/28/23 21:36 V30280MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 02/28/23 21:36 V30280MSA
9000 µg/L 110 250Toluene 500 03/02/23 03:11 V30431MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 02/28/23 21:36 V30280MSA
<3.10 µg/L 3.10 5.00
1,2,4-Trichlorobenzene 10 02/28/23 21:36 V30280MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 02/28/23 21:36 V30280MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 02/28/23 21:36 V30280MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 02/28/23 21:36 V30280MSA
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 02/28/23 21:36 V30280MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 02/28/23 21:36 V30280MSA
905 µg/L 95.0 2501,2,4-Trimethylbenzene 500 03/02/23 03:11 V30431MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-9
89753 Matrix:
2/23/2023 14:06
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00 V30429 03/01/23 09:00
293 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 02/28/23 21:36 V30280MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 02/28/23 21:36 V30280MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 02/28/23 21:36 V30280MSA
1740 µg/L 105 250o-Xylene 500 03/02/23 03:11 V30431MSA
3790 µg/L 210 500m,p-Xylene 500 03/02/23 03:11 V30431MSA
5530 µg/L 105 250Xylene (Total)500 03/02/23 03:11 V30431
Surrogate: 4-Bromofluorobenzene 95.8 Limits: 70-130%02/28/23 21:3610 MSA V30280
Surrogate: Dibromofluoromethane 84.2 Limits: 70-130%02/28/23 21:3610 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 120 Limits: 70-130%02/28/23 21:3610 MSA V30280
Surrogate: Toluene-d8 98.6 Limits: 70-130%02/28/23 21:3610 MSA V30280
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%03/02/23 03:11500 MSA V30431
Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%03/02/23 03:11500 MSA V30431
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%03/02/23 03:11500 MSA V30431
Surrogate: Toluene-d8 99.6 Limits: 70-130%03/02/23 03:11500 MSA V30431
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-10
89754 Matrix:
2/23/2023 12:31
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 02/28/23 19:10 6200BMSA
Surrogate: 4-Bromofluorobenzene 96.6 Limits: 70-130%02/28/23 19:101 MSA V30280
Surrogate: Dibromofluoromethane 88.0 Limits: 70-130%02/28/23 19:101 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 112 Limits: 70-130%02/28/23 19:101 MSA V30280
Surrogate: Toluene-d8 104 Limits: 70-130%02/28/23 19:101 MSA V30280
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%03/02/23 01:58100 MSA V30431
Surrogate: Dibromofluoromethane 99.8 Limits: 70-130%03/02/23 01:58100 MSA V30431
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%03/02/23 01:58100 MSA V30431
Surrogate: Toluene-d8 99.8 Limits: 70-130%03/02/23 01:58100 MSA V30431
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-10
89754 Matrix:
2/23/2023 12:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00 V30429 03/01/23 09:00
68.8 µg/L 1.80 10.0Acetone 1 02/28/23 19:10 V30280MSA
95.1 µg/L 0.180 0.500Benzene 1 02/28/23 19:10 V30280MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/28/23 19:10 V30280MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/28/23 19:10 V30280MSA
5.03 µg/L 0.160 0.500Bromodichloromethane 1 02/28/23 19:10 V30280MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/28/23 19:10 V30280MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/28/23 19:10 V30280MSA
0.474 J µg/L 0.180 0.500n-Butylbenzene 1 02/28/23 19:10 V30280MSA
0.373 J
µg/L 0.200 0.500
sec-Butyl benzene 1 02/28/23 19:10 V30280MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/28/23 19:10 V30280MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/28/23 19:10 V30280MSA
5.42 µg/L 0.190 0.500Chlorobenzene 1 02/28/23 19:10 V30280MSA
2.99 µg/L 0.190 0.500Chlorodibromomethane 1 02/28/23 19:10 V30280MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/28/23 19:10 V30280MSA
43.7 µg/L 0.220 0.500Chloroform 1 02/28/23 19:10 V30280MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 02/28/23 19:10 V30280MSA
2.75 µg/L 0.200 0.5002-Chlorotoluene 1 02/28/23 19:10 V30280MSA
1.65 µg/L 0.200 0.5004-Chlorotoluene 1 02/28/23 19:10 V30280MSA
80.4 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 02/28/23 19:10 V30280MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/28/23 19:10 V30280MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/28/23 19:10 V30280MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/28/23 19:10 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-10
89754 Matrix:
2/23/2023 12:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00 V30429 03/01/23 09:00
1.77 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/28/23 19:10 V30280MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/28/23 19:10 V30280MSA
5.77 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/28/23 19:10 V30280MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/28/23 19:10 V30280MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/28/23 19:10 V30280MSA
13.3 µg/L 0.150 0.5001,2-Dichloroethane 1 02/28/23 19:10 V30280MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/28/23 19:10 V30280MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/28/23 19:10 V30280MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 02/28/23 19:10 V30280MSA
1.63 µg/L 0.190 0.5001,2-Dichloropropane 1 02/28/23 19:10 V30280MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/28/23 19:10 V30280MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/28/23 19:10 V30280MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/28/23 19:10 V30280MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/28/23 19:10 V30280MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/28/23 19:10 V30280MSA
<42.0 µg/L 42.0 200
Ethanol 1 02/28/23 19:10 V30280MSA
19.7 µg/L 0.170 0.500Ethylbenzene 1 02/28/23 19:10 V30280MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 02/28/23 19:10 V30280MSA
8.38 µg/L 0.380 1.002-Hexanone 1 02/28/23 19:10 V30280MSA
1.81 µg/L 0.180 0.500Isopropylbenzene 1 02/28/23 19:10 V30280MSA
0.371 J µg/L 0.089 0.5004-Isopropyl toluene 1 02/28/23 19:10 V30280MSA
45.1 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/28/23 19:10 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-10
89754 Matrix:
2/23/2023 12:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00 V30429 03/01/23 09:00
207 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 03/02/23 01:58 V30431MSA
10.6 µg/L 0.078 1.004-Methyl-2-Pentanone 1 02/28/23 19:10 V30280MSA
2.70 µg/L 0.330 2.00Methylene Chloride 1 02/28/23 19:10 V30280MSA
9.45 µg/L 0.470 1.00Naphthalene 1 02/28/23 19:10 V30280MSA
3.22 µg/L 0.190 0.500n-Propylbenzene 1 02/28/23 19:10 V30280MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/28/23 19:10 V30280MSA
199 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 02/28/23 19:10 V30280MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 02/28/23 19:10 V30280MSA
1100 µg/L 190 1000
tert-Amyl Alcohol (TAA)100 03/02/23 01:58 V30431MSA
7.84 J µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 02/28/23 19:10 V30280MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/28/23 19:10 V30280MSA
1.18 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/28/23 19:10 V30280MSA
0.561 µg/L 0.220 0.500Tetrachloroethene 1 02/28/23 19:10 V30280MSA
22.1 µg/L 0.220 0.500Toluene 1 02/28/23 19:10 V30280MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 02/28/23 19:10 V30280MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 02/28/23 19:10 V30280MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/28/23 19:10 V30280MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/28/23 19:10 V30280MSA
0.384 J µg/L 0.180 0.500Trichloroethene 1 02/28/23 19:10 V30280MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/28/23 19:10 V30280MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 02/28/23 19:10 V30280MSA
46.0 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 02/28/23 19:10 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-10
89754 Matrix:
2/23/2023 12:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00 V30429 03/01/23 09:00
3.94 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/28/23 19:10 V30280MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 02/28/23 19:10 V30280MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/28/23 19:10 V30280MSA
66.3 µg/L 0.210 0.500o-Xylene 1 02/28/23 19:10 V30280MSA
146 µg/L 0.420 1.00m,p-Xylene 1 02/28/23 19:10 V30280MSA
212 µg/L 0.210 0.500Xylene (Total)1 02/28/23 19:10 V30280
Surrogate: 4-Bromofluorobenzene 96.6 Limits: 70-130%02/28/23 19:101 MSA V30280
Surrogate: Dibromofluoromethane 88.0 Limits: 70-130%02/28/23 19:101 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 112 Limits: 70-130%02/28/23 19:101 MSA V30280
Surrogate: Toluene-d8 104 Limits: 70-130%02/28/23 19:101 MSA V30280
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%03/02/23 01:58100 MSA V30431
Surrogate: Dibromofluoromethane 99.8 Limits: 70-130%03/02/23 01:58100 MSA V30431
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%03/02/23 01:58100 MSA V30431
Surrogate: Toluene-d8 99.8 Limits: 70-130%03/02/23 01:58100 MSA V30431
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-11
89755 Matrix:
2/23/2023 12:41
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 02/28/23 18:22 6200BMSA
Surrogate: 4-Bromofluorobenzene 93.8 Limits: 70-130%02/28/23 18:221 MSA V30280
Surrogate: Dibromofluoromethane 94.6 Limits: 70-130%02/28/23 18:221 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%02/28/23 18:221 MSA V30280
Surrogate: Toluene-d8 103 Limits: 70-130%02/28/23 18:221 MSA V30280
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 53 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-11
89755 Matrix:
2/23/2023 12:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 02/28/23 18:22 V30280MSA
19.0 µg/L 0.180 0.500Benzene 1 02/28/23 18:22 V30280MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/28/23 18:22 V30280MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/28/23 18:22 V30280MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/28/23 18:22 V30280MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/28/23 18:22 V30280MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/28/23 18:22 V30280MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 02/28/23 18:22 V30280MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 02/28/23 18:22 V30280MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/28/23 18:22 V30280MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/28/23 18:22 V30280MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/28/23 18:22 V30280MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/28/23 18:22 V30280MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/28/23 18:22 V30280MSA
<0.220 µg/L 0.220 0.500Chloroform 1 02/28/23 18:22 V30280MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 02/28/23 18:22 V30280MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/28/23 18:22 V30280MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/28/23 18:22 V30280MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 02/28/23 18:22 V30280MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/28/23 18:22 V30280MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/28/23 18:22 V30280MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/28/23 18:22 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 54 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-11
89755 Matrix:
2/23/2023 12:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/28/23 18:22 V30280MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/28/23 18:22 V30280MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/28/23 18:22 V30280MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/28/23 18:22 V30280MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/28/23 18:22 V30280MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/28/23 18:22 V30280MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/28/23 18:22 V30280MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/28/23 18:22 V30280MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 02/28/23 18:22 V30280MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/28/23 18:22 V30280MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/28/23 18:22 V30280MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/28/23 18:22 V30280MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/28/23 18:22 V30280MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/28/23 18:22 V30280MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/28/23 18:22 V30280MSA
<42.0 µg/L 42.0 200
Ethanol 1 02/28/23 18:22 V30280MSA
0.648 µg/L 0.170 0.500Ethylbenzene 1 02/28/23 18:22 V30280MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 02/28/23 18:22 V30280MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 02/28/23 18:22 V30280MSA
0.533 µg/L 0.180 0.500Isopropylbenzene 1 02/28/23 18:22 V30280MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/28/23 18:22 V30280MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/28/23 18:22 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 55 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-11
89755 Matrix:
2/23/2023 12:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 02/28/23 18:22 V30280MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 02/28/23 18:22 V30280MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 02/28/23 18:22 V30280MSA
1.32 µg/L 0.470 1.00Naphthalene 1 02/28/23 18:22 V30280MSA
0.533 µg/L 0.190 0.500n-Propylbenzene 1 02/28/23 18:22 V30280MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/28/23 18:22 V30280MSA
86.1 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 02/28/23 18:22 V30280MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 02/28/23 18:22 V30280MSA
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 02/28/23 18:22 V30280MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 02/28/23 18:22 V30280MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/28/23 18:22 V30280MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/28/23 18:22 V30280MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/28/23 18:22 V30280MSA
<0.220 µg/L 0.220 0.500Toluene 1 02/28/23 18:22 V30280MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 02/28/23 18:22 V30280MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 02/28/23 18:22 V30280MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/28/23 18:22 V30280MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/28/23 18:22 V30280MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/28/23 18:22 V30280MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/28/23 18:22 V30280MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 02/28/23 18:22 V30280MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 02/28/23 18:22 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 56 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-11
89755 Matrix:
2/23/2023 12:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/28/23 18:22 V30280MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 02/28/23 18:22 V30280MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/28/23 18:22 V30280MSA
1.54 µg/L 0.210 0.500o-Xylene 1 02/28/23 18:22 V30280MSA
7.26 µg/L 0.420 1.00m,p-Xylene 1 02/28/23 18:22 V30280MSA
8.80 µg/L 0.210 0.500Xylene (Total)1 02/28/23 18:22 V30280
Surrogate: 4-Bromofluorobenzene 93.8 Limits: 70-130%02/28/23 18:221 MSA V30280
Surrogate: Dibromofluoromethane 94.6 Limits: 70-130%02/28/23 18:221 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%02/28/23 18:221 MSA V30280
Surrogate: Toluene-d8 103 Limits: 70-130%02/28/23 18:221 MSA V30280
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 57 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-12
89756 Matrix:
2/23/2023 12:20
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 02/28/23 18:46 6200BMSA
Surrogate: 4-Bromofluorobenzene 95.6 Limits: 70-130%02/28/23 18:461 MSA V30280
Surrogate: Dibromofluoromethane 99.0 Limits: 70-130%02/28/23 18:461 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%02/28/23 18:461 MSA V30280
Surrogate: Toluene-d8 106 Limits: 70-130%02/28/23 18:461 MSA V30280
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 58 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-12
89756 Matrix:
2/23/2023 12:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 02/28/23 18:46 V30280MSA
0.658 µg/L 0.180 0.500Benzene 1 02/28/23 18:46 V30280MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/28/23 18:46 V30280MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/28/23 18:46 V30280MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/28/23 18:46 V30280MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/28/23 18:46 V30280MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/28/23 18:46 V30280MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 02/28/23 18:46 V30280MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 02/28/23 18:46 V30280MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/28/23 18:46 V30280MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/28/23 18:46 V30280MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/28/23 18:46 V30280MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/28/23 18:46 V30280MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/28/23 18:46 V30280MSA
1.55 µg/L 0.220 0.500Chloroform 1 02/28/23 18:46 V30280MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 02/28/23 18:46 V30280MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/28/23 18:46 V30280MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/28/23 18:46 V30280MSA
4.17 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 02/28/23 18:46 V30280MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/28/23 18:46 V30280MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/28/23 18:46 V30280MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/28/23 18:46 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 59 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-12
89756 Matrix:
2/23/2023 12:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/28/23 18:46 V30280MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/28/23 18:46 V30280MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/28/23 18:46 V30280MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/28/23 18:46 V30280MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/28/23 18:46 V30280MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/28/23 18:46 V30280MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/28/23 18:46 V30280MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/28/23 18:46 V30280MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 02/28/23 18:46 V30280MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/28/23 18:46 V30280MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/28/23 18:46 V30280MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/28/23 18:46 V30280MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/28/23 18:46 V30280MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/28/23 18:46 V30280MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/28/23 18:46 V30280MSA
<42.0 µg/L 42.0 200
Ethanol 1 02/28/23 18:46 V30280MSA
0.597 µg/L 0.170 0.500Ethylbenzene 1 02/28/23 18:46 V30280MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 02/28/23 18:46 V30280MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 02/28/23 18:46 V30280MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 02/28/23 18:46 V30280MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/28/23 18:46 V30280MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/28/23 18:46 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 60 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-12
89756 Matrix:
2/23/2023 12:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
57.6 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 02/28/23 18:46 V30280MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 02/28/23 18:46 V30280MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 02/28/23 18:46 V30280MSA
1.15 µg/L 0.470 1.00Naphthalene 1 02/28/23 18:46 V30280MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 02/28/23 18:46 V30280MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/28/23 18:46 V30280MSA
55.3 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 02/28/23 18:46 V30280MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 02/28/23 18:46 V30280MSA
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 02/28/23 18:46 V30280MSA
2.57 J µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 02/28/23 18:46 V30280MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/28/23 18:46 V30280MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/28/23 18:46 V30280MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/28/23 18:46 V30280MSA
<0.220 µg/L 0.220 0.500Toluene 1 02/28/23 18:46 V30280MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 02/28/23 18:46 V30280MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 02/28/23 18:46 V30280MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/28/23 18:46 V30280MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/28/23 18:46 V30280MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/28/23 18:46 V30280MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/28/23 18:46 V30280MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 02/28/23 18:46 V30280MSA
0.761 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 02/28/23 18:46 V30280MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 61 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-12
89756 Matrix:
2/23/2023 12:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30279 02/28/23 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/28/23 18:46 V30280MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 02/28/23 18:46 V30280MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/28/23 18:46 V30280MSA
2.15 µg/L 0.210 0.500o-Xylene 1 02/28/23 18:46 V30280MSA
3.85 µg/L 0.420 1.00m,p-Xylene 1 02/28/23 18:46 V30280MSA
6.00 µg/L 0.210 0.500Xylene (Total)1 02/28/23 18:46 V30280
Surrogate: 4-Bromofluorobenzene 95.6 Limits: 70-130%02/28/23 18:461 MSA V30280
Surrogate: Dibromofluoromethane 99.0 Limits: 70-130%02/28/23 18:461 MSA V30280
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%02/28/23 18:461 MSA V30280
Surrogate: Toluene-d8 106 Limits: 70-130%02/28/23 18:461 MSA V30280
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 62 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-13
89757 Matrix:
2/23/2023 11:44
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 03/01/23 02:29 6200BMSA
Surrogate: 4-Bromofluorobenzene 92.2 Limits: 70-130%03/01/23 02:291 MSA V30378
Surrogate: Dibromofluoromethane 99.2 Limits: 70-130%03/01/23 02:291 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%03/01/23 02:291 MSA V30378
Surrogate: Toluene-d8 107 Limits: 70-130%03/01/23 02:291 MSA V30378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 63 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-13
89757 Matrix:
2/23/2023 11:44
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 03/01/23 02:29 V30378MSA
<0.180 µg/L 0.180 0.500Benzene 1 03/01/23 02:29 V30378MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 03/01/23 02:29 V30378MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 03/01/23 02:29 V30378MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 03/01/23 02:29 V30378MSA
<1.50 µg/L 1.50 5.00Bromoform 1 03/01/23 02:29 V30378MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 03/01/23 02:29 V30378MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 03/01/23 02:29 V30378MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 03/01/23 02:29 V30378MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 03/01/23 02:29 V30378MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 03/01/23 02:29 V30378MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 03/01/23 02:29 V30378MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 03/01/23 02:29 V30378MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 03/01/23 02:29 V30378MSA
<0.220 µg/L 0.220 0.500Chloroform 1 03/01/23 02:29 V30378MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 03/01/23 02:29 V30378MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 03/01/23 02:29 V30378MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 03/01/23 02:29 V30378MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 03/01/23 02:29 V30378MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 03/01/23 02:29 V30378MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 03/01/23 02:29 V30378MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 03/01/23 02:29 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 64 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-13
89757 Matrix:
2/23/2023 11:44
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 03/01/23 02:29 V30378MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 03/01/23 02:29 V30378MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 03/01/23 02:29 V30378MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 03/01/23 02:29 V30378MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 03/01/23 02:29 V30378MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 03/01/23 02:29 V30378MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 03/01/23 02:29 V30378MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 03/01/23 02:29 V30378MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 03/01/23 02:29 V30378MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 03/01/23 02:29 V30378MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 03/01/23 02:29 V30378MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 03/01/23 02:29 V30378MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 03/01/23 02:29 V30378MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 03/01/23 02:29 V30378MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 03/01/23 02:29 V30378MSA
<42.0 µg/L 42.0 200
Ethanol 1 03/01/23 02:29 V30378MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 03/01/23 02:29 V30378MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 03/01/23 02:29 V30378MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 03/01/23 02:29 V30378MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 03/01/23 02:29 V30378MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 03/01/23 02:29 V30378MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 03/01/23 02:29 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 65 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-13
89757 Matrix:
2/23/2023 11:44
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 03/01/23 02:29 V30378MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 03/01/23 02:29 V30378MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 03/01/23 02:29 V30378MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 03/01/23 02:29 V30378MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 03/01/23 02:29 V30378MSA
<0.220 µg/L 0.220 0.500Styrene 1 03/01/23 02:29 V30378MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 03/01/23 02:29 V30378MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 03/01/23 02:29 V30378MSA
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 03/01/23 02:29 V30378MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 03/01/23 02:29 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 03/01/23 02:29 V30378MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 03/01/23 02:29 V30378MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 03/01/23 02:29 V30378MSA
<0.220 µg/L 0.220 0.500Toluene 1 03/01/23 02:29 V30378MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 03/01/23 02:29 V30378MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 03/01/23 02:29 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 03/01/23 02:29 V30378MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 03/01/23 02:29 V30378MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 03/01/23 02:29 V30378MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 03/01/23 02:29 V30378MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 03/01/23 02:29 V30378MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 03/01/23 02:29 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 66 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-13
89757 Matrix:
2/23/2023 11:44
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 03/01/23 02:29 V30378MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 03/01/23 02:29 V30378MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 03/01/23 02:29 V30378MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 03/01/23 02:29 V30378MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 03/01/23 02:29 V30378MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 03/01/23 02:29 V30378
Surrogate: 4-Bromofluorobenzene 92.2 Limits: 70-130%03/01/23 02:291 MSA V30378
Surrogate: Dibromofluoromethane 99.2 Limits: 70-130%03/01/23 02:291 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%03/01/23 02:291 MSA V30378
Surrogate: Toluene-d8 107 Limits: 70-130%03/01/23 02:291 MSA V30378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 67 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-14
89758 Matrix:
2/23/2023 11:18
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 03/01/23 02:54 6200BMSA
Surrogate: 4-Bromofluorobenzene 96.0 Limits: 70-130%03/01/23 02:541 MSA V30378
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%03/01/23 02:541 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%03/01/23 02:541 MSA V30378
Surrogate: Toluene-d8 108 Limits: 70-130%03/01/23 02:541 MSA V30378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 68 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-14
89758 Matrix:
2/23/2023 11:18
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 03/01/23 02:54 V30378MSA
<0.180 µg/L 0.180 0.500Benzene 1 03/01/23 02:54 V30378MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 03/01/23 02:54 V30378MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 03/01/23 02:54 V30378MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 03/01/23 02:54 V30378MSA
<1.50 µg/L 1.50 5.00Bromoform 1 03/01/23 02:54 V30378MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 03/01/23 02:54 V30378MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 03/01/23 02:54 V30378MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 03/01/23 02:54 V30378MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 03/01/23 02:54 V30378MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 03/01/23 02:54 V30378MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 03/01/23 02:54 V30378MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 03/01/23 02:54 V30378MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 03/01/23 02:54 V30378MSA
1.02 µg/L 0.220 0.500Chloroform 1 03/01/23 02:54 V30378MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 03/01/23 02:54 V30378MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 03/01/23 02:54 V30378MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 03/01/23 02:54 V30378MSA
1.53 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 03/01/23 02:54 V30378MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 03/01/23 02:54 V30378MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 03/01/23 02:54 V30378MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 03/01/23 02:54 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 69 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-14
89758 Matrix:
2/23/2023 11:18
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 03/01/23 02:54 V30378MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 03/01/23 02:54 V30378MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 03/01/23 02:54 V30378MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 03/01/23 02:54 V30378MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 03/01/23 02:54 V30378MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 03/01/23 02:54 V30378MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 03/01/23 02:54 V30378MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 03/01/23 02:54 V30378MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 03/01/23 02:54 V30378MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 03/01/23 02:54 V30378MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 03/01/23 02:54 V30378MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 03/01/23 02:54 V30378MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 03/01/23 02:54 V30378MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 03/01/23 02:54 V30378MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 03/01/23 02:54 V30378MSA
<42.0 µg/L 42.0 200
Ethanol 1 03/01/23 02:54 V30378MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 03/01/23 02:54 V30378MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 03/01/23 02:54 V30378MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 03/01/23 02:54 V30378MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 03/01/23 02:54 V30378MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 03/01/23 02:54 V30378MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 03/01/23 02:54 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 70 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-14
89758 Matrix:
2/23/2023 11:18
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
1.62 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 03/01/23 02:54 V30378MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 03/01/23 02:54 V30378MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 03/01/23 02:54 V30378MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 03/01/23 02:54 V30378MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 03/01/23 02:54 V30378MSA
<0.220 µg/L 0.220 0.500Styrene 1 03/01/23 02:54 V30378MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 03/01/23 02:54 V30378MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 03/01/23 02:54 V30378MSA
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 03/01/23 02:54 V30378MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 03/01/23 02:54 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 03/01/23 02:54 V30378MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 03/01/23 02:54 V30378MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 03/01/23 02:54 V30378MSA
<0.220 µg/L 0.220 0.500Toluene 1 03/01/23 02:54 V30378MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 03/01/23 02:54 V30378MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 03/01/23 02:54 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 03/01/23 02:54 V30378MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 03/01/23 02:54 V30378MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 03/01/23 02:54 V30378MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 03/01/23 02:54 V30378MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 03/01/23 02:54 V30378MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 03/01/23 02:54 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 71 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-14
89758 Matrix:
2/23/2023 11:18
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 03/01/23 02:54 V30378MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 03/01/23 02:54 V30378MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 03/01/23 02:54 V30378MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 03/01/23 02:54 V30378MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 03/01/23 02:54 V30378MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 03/01/23 02:54 V30378
Surrogate: 4-Bromofluorobenzene 96.0 Limits: 70-130%03/01/23 02:541 MSA V30378
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%03/01/23 02:541 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%03/01/23 02:541 MSA V30378
Surrogate: Toluene-d8 108 Limits: 70-130%03/01/23 02:541 MSA V30378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 72 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-15
89759 Matrix:
2/23/2023 11:31
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 03/01/23 07:22 6200BMSA
Surrogate: 4-Bromofluorobenzene 97.6 Limits: 70-130%03/01/23 07:22100 MSA V30378
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%03/01/23 07:22100 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 108 Limits: 70-130%03/01/23 07:22100 MSA V30378
Surrogate: Toluene-d8 101 Limits: 70-130%03/01/23 07:22100 MSA V30378
Surrogate: 4-Bromofluorobenzene 94.4 Limits: 70-130%03/07/23 09:14100 MSA V30528
Surrogate: Dibromofluoromethane 100 Limits: 70-130%03/07/23 09:14100 MSA V30528
Surrogate: 1,2-Dichloroethane - d4 85.4 Limits: 70-130%03/07/23 09:14100 MSA V30528
Surrogate: Toluene-d8 94.0 Limits: 70-130%03/07/23 09:14100 MSA V30528
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 73 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-15
89759 Matrix:
2/23/2023 11:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00 V30526 03/06/23 14:00
<180 µg/L 180 1000Acetone 100 03/01/23 07:22 V30378MSA
7610 µg/L 18.0 50.0Benzene 100 03/01/23 07:22 V30378MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 03/01/23 07:22 V30378MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 03/01/23 07:22 V30378MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 03/01/23 07:22 V30378MSA
<150 µg/L 150 500Bromoform 100 03/01/23 07:22 V30378MSA
<28.0 µg/L 28.0 100Bromomethane 100 03/01/23 07:22 V30378MSA
<18.0 µg/L 18.0 50.0n-Butylbenzene 100 03/01/23 07:22 V30378MSA
<20.0 µg/L 20.0 50.0
sec-Butyl benzene 100 03/01/23 07:22 V30378MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 03/01/23 07:22 V30378MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 03/01/23 07:22 V30378MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 03/01/23 07:22 V30378MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 03/01/23 07:22 V30378MSA
<43.0 µg/L 43.0 100Chloroethane 100 03/01/23 07:22 V30378MSA
<22.0 µg/L 22.0 50.0Chloroform 100 03/01/23 07:22 V30378MSA
<22.0 µg/L 22.0 50.0
Chloromethane 100 03/01/23 07:22 V30378MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 03/01/23 07:22 V30378MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 03/01/23 07:22 V30378MSA
884 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 03/01/23 07:22 V30378MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 03/01/23 07:22 V30378MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 03/01/23 07:22 V30378MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 03/01/23 07:22 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 74 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-15
89759 Matrix:
2/23/2023 11:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00 V30526 03/06/23 14:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 03/01/23 07:22 V30378MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 03/01/23 07:22 V30378MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 03/01/23 07:22 V30378MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 03/01/23 07:22 V30378MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 03/01/23 07:22 V30378MSA
199 µg/L 15.0 50.01,2-Dichloroethane 100 03/01/23 07:22 V30378MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 03/01/23 07:22 V30378MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 03/01/23 07:22 V30378MSA
<18.0 µg/L 18.0 50.0
trans-1,2-Dichloroethene 100 03/01/23 07:22 V30378MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 03/01/23 07:22 V30378MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 03/01/23 07:22 V30378MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 03/01/23 07:22 V30378MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 03/01/23 07:22 V30378MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 03/01/23 07:22 V30378MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 03/01/23 07:22 V30378MSA
67600 µg/L 4200 20000
Ethanol 100 03/01/23 07:22 V30378MSA
985 µg/L 17.0 50.0Ethylbenzene 100 03/01/23 07:22 V30378MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 03/01/23 07:22 V30378MSA
<38.0 µg/L 38.0 1002-Hexanone 100 03/01/23 07:22 V30378MSA
36.4 J µg/L 18.0 50.0Isopropylbenzene 100 03/01/23 07:22 V30378MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 03/01/23 07:22 V30378MSA
586 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 03/01/23 07:22 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 75 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-15
89759 Matrix:
2/23/2023 11:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00 V30526 03/06/23 14:00
1280 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 03/01/23 07:22 V30378MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 03/01/23 07:22 V30378MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 03/01/23 07:22 V30378MSA
422 µg/L 47.0 100Naphthalene 100 03/01/23 07:22 V30378MSA
104 µg/L 19.0 50.0n-Propylbenzene 100 03/01/23 07:22 V30378MSA
<22.0 µg/L 22.0 50.0Styrene 100 03/01/23 07:22 V30378MSA
1350 µg/L 160 1000tert-Butyl Alcohol (TBA)100 03/01/23 07:22 V30378MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 03/01/23 07:22 V30378MSA
4170 µg/L 190 1000
tert-Amyl Alcohol (TAA)100 03/01/23 07:22 V30378MSA
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 03/01/23 07:22 V30378MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 03/01/23 07:22 V30378MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 03/01/23 07:22 V30378MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 03/01/23 07:22 V30378MSA
8480 µg/L 22.0 50.0Toluene 100 03/07/23 09:14 V30528MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 03/01/23 07:22 V30378MSA
<31.0 µg/L 31.0 50.0
1,2,4-Trichlorobenzene 100 03/01/23 07:22 V30378MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 03/01/23 07:22 V30378MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 03/01/23 07:22 V30378MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 03/01/23 07:22 V30378MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 03/01/23 07:22 V30378MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 03/01/23 07:22 V30378MSA
694 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 03/01/23 07:22 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 76 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-15
89759 Matrix:
2/23/2023 11:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00 V30526 03/06/23 14:00
231 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 03/01/23 07:22 V30378MSA
<100 µg/L 100 500Vinyl Acetate 100 03/01/23 07:22 V30378MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 03/01/23 07:22 V30378MSA
1320 µg/L 21.0 50.0o-Xylene 100 03/01/23 07:22 V30378MSA
3400 µg/L 42.0 100m,p-Xylene 100 03/01/23 07:22 V30378MSA
4720 µg/L 21.0 50.0Xylene (Total)100 03/01/23 07:22 V30378
Surrogate: 4-Bromofluorobenzene 97.6 Limits: 70-130%03/01/23 07:22100 MSA V30378
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%03/01/23 07:22100 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 108 Limits: 70-130%03/01/23 07:22100 MSA V30378
Surrogate: Toluene-d8 101 Limits: 70-130%03/01/23 07:22100 MSA V30378
Surrogate: 4-Bromofluorobenzene 94.4 Limits: 70-130%03/07/23 09:14100 MSA V30528
Surrogate: Dibromofluoromethane 100 Limits: 70-130%03/07/23 09:14100 MSA V30528
Surrogate: 1,2-Dichloroethane - d4 85.4 Limits: 70-130%03/07/23 09:14100 MSA V30528
Surrogate: Toluene-d8 94.0 Limits: 70-130%03/07/23 09:14100 MSA V30528
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 77 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-16
89760 Matrix:
2/23/2023 11:06
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 03/01/23 03:18 6200BMSA
Surrogate: 4-Bromofluorobenzene 92.4 Limits: 70-130%03/01/23 03:181 MSA V30378
Surrogate: Dibromofluoromethane 99.4 Limits: 70-130%03/01/23 03:181 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%03/01/23 03:181 MSA V30378
Surrogate: Toluene-d8 107 Limits: 70-130%03/01/23 03:181 MSA V30378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 78 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-16
89760 Matrix:
2/23/2023 11:06
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 03/01/23 03:18 V30378MSA
<0.180 µg/L 0.180 0.500Benzene 1 03/01/23 03:18 V30378MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 03/01/23 03:18 V30378MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 03/01/23 03:18 V30378MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 03/01/23 03:18 V30378MSA
<1.50 µg/L 1.50 5.00Bromoform 1 03/01/23 03:18 V30378MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 03/01/23 03:18 V30378MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 03/01/23 03:18 V30378MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 03/01/23 03:18 V30378MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 03/01/23 03:18 V30378MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 03/01/23 03:18 V30378MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 03/01/23 03:18 V30378MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 03/01/23 03:18 V30378MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 03/01/23 03:18 V30378MSA
<0.220 µg/L 0.220 0.500Chloroform 1 03/01/23 03:18 V30378MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 03/01/23 03:18 V30378MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 03/01/23 03:18 V30378MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 03/01/23 03:18 V30378MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 03/01/23 03:18 V30378MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 03/01/23 03:18 V30378MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 03/01/23 03:18 V30378MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 03/01/23 03:18 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 79 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-16
89760 Matrix:
2/23/2023 11:06
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 03/01/23 03:18 V30378MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 03/01/23 03:18 V30378MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 03/01/23 03:18 V30378MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 03/01/23 03:18 V30378MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 03/01/23 03:18 V30378MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 03/01/23 03:18 V30378MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 03/01/23 03:18 V30378MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 03/01/23 03:18 V30378MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 03/01/23 03:18 V30378MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 03/01/23 03:18 V30378MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 03/01/23 03:18 V30378MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 03/01/23 03:18 V30378MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 03/01/23 03:18 V30378MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 03/01/23 03:18 V30378MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 03/01/23 03:18 V30378MSA
<42.0 µg/L 42.0 200
Ethanol 1 03/01/23 03:18 V30378MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 03/01/23 03:18 V30378MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 03/01/23 03:18 V30378MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 03/01/23 03:18 V30378MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 03/01/23 03:18 V30378MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 03/01/23 03:18 V30378MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 03/01/23 03:18 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 80 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-16
89760 Matrix:
2/23/2023 11:06
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 03/01/23 03:18 V30378MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 03/01/23 03:18 V30378MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 03/01/23 03:18 V30378MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 03/01/23 03:18 V30378MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 03/01/23 03:18 V30378MSA
<0.220 µg/L 0.220 0.500Styrene 1 03/01/23 03:18 V30378MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 03/01/23 03:18 V30378MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 03/01/23 03:18 V30378MSA
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 03/01/23 03:18 V30378MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 03/01/23 03:18 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 03/01/23 03:18 V30378MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 03/01/23 03:18 V30378MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 03/01/23 03:18 V30378MSA
<0.220 µg/L 0.220 0.500Toluene 1 03/01/23 03:18 V30378MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 03/01/23 03:18 V30378MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 03/01/23 03:18 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 03/01/23 03:18 V30378MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 03/01/23 03:18 V30378MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 03/01/23 03:18 V30378MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 03/01/23 03:18 V30378MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 03/01/23 03:18 V30378MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 03/01/23 03:18 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 81 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-16
89760 Matrix:
2/23/2023 11:06
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 03/01/23 03:18 V30378MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 03/01/23 03:18 V30378MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 03/01/23 03:18 V30378MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 03/01/23 03:18 V30378MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 03/01/23 03:18 V30378MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 03/01/23 03:18 V30378
Surrogate: 4-Bromofluorobenzene 92.4 Limits: 70-130%03/01/23 03:181 MSA V30378
Surrogate: Dibromofluoromethane 99.4 Limits: 70-130%03/01/23 03:181 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%03/01/23 03:181 MSA V30378
Surrogate: Toluene-d8 107 Limits: 70-130%03/01/23 03:181 MSA V30378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 82 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-17
89761 Matrix:
2/23/2023 10:55
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 03/01/23 03:42 6200BMSA
Surrogate: 4-Bromofluorobenzene 92.6 Limits: 70-130%03/01/23 03:421 MSA V30378
Surrogate: Dibromofluoromethane 103 Limits: 70-130%03/01/23 03:421 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%03/01/23 03:421 MSA V30378
Surrogate: Toluene-d8 106 Limits: 70-130%03/01/23 03:421 MSA V30378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 83 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-17
89761 Matrix:
2/23/2023 10:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
2.92 J µg/L 1.80 10.0Acetone 1 03/01/23 03:42 V30378MSA
<0.180 µg/L 0.180 0.500Benzene 1 03/01/23 03:42 V30378MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 03/01/23 03:42 V30378MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 03/01/23 03:42 V30378MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 03/01/23 03:42 V30378MSA
<1.50 µg/L 1.50 5.00Bromoform 1 03/01/23 03:42 V30378MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 03/01/23 03:42 V30378MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 03/01/23 03:42 V30378MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 03/01/23 03:42 V30378MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 03/01/23 03:42 V30378MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 03/01/23 03:42 V30378MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 03/01/23 03:42 V30378MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 03/01/23 03:42 V30378MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 03/01/23 03:42 V30378MSA
<0.220 µg/L 0.220 0.500Chloroform 1 03/01/23 03:42 V30378MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 03/01/23 03:42 V30378MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 03/01/23 03:42 V30378MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 03/01/23 03:42 V30378MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 03/01/23 03:42 V30378MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 03/01/23 03:42 V30378MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 03/01/23 03:42 V30378MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 03/01/23 03:42 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 84 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-17
89761 Matrix:
2/23/2023 10:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 03/01/23 03:42 V30378MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 03/01/23 03:42 V30378MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 03/01/23 03:42 V30378MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 03/01/23 03:42 V30378MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 03/01/23 03:42 V30378MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 03/01/23 03:42 V30378MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 03/01/23 03:42 V30378MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 03/01/23 03:42 V30378MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 03/01/23 03:42 V30378MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 03/01/23 03:42 V30378MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 03/01/23 03:42 V30378MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 03/01/23 03:42 V30378MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 03/01/23 03:42 V30378MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 03/01/23 03:42 V30378MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 03/01/23 03:42 V30378MSA
<42.0 µg/L 42.0 200
Ethanol 1 03/01/23 03:42 V30378MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 03/01/23 03:42 V30378MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 03/01/23 03:42 V30378MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 03/01/23 03:42 V30378MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 03/01/23 03:42 V30378MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 03/01/23 03:42 V30378MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 03/01/23 03:42 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 85 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-17
89761 Matrix:
2/23/2023 10:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 03/01/23 03:42 V30378MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 03/01/23 03:42 V30378MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 03/01/23 03:42 V30378MSA
1.07 µg/L 0.470 1.00Naphthalene 1 03/01/23 03:42 V30378MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 03/01/23 03:42 V30378MSA
<0.220 µg/L 0.220 0.500Styrene 1 03/01/23 03:42 V30378MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 03/01/23 03:42 V30378MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 03/01/23 03:42 V30378MSA
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 03/01/23 03:42 V30378MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 03/01/23 03:42 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 03/01/23 03:42 V30378MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 03/01/23 03:42 V30378MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 03/01/23 03:42 V30378MSA
2.21 µg/L 0.220 0.500Toluene 1 03/01/23 03:42 V30378MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 03/01/23 03:42 V30378MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 03/01/23 03:42 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 03/01/23 03:42 V30378MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 03/01/23 03:42 V30378MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 03/01/23 03:42 V30378MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 03/01/23 03:42 V30378MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 03/01/23 03:42 V30378MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 03/01/23 03:42 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 86 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-17
89761 Matrix:
2/23/2023 10:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 03/01/23 03:42 V30378MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 03/01/23 03:42 V30378MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 03/01/23 03:42 V30378MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 03/01/23 03:42 V30378MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 03/01/23 03:42 V30378MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 03/01/23 03:42 V30378
Surrogate: 4-Bromofluorobenzene 92.6 Limits: 70-130%03/01/23 03:421 MSA V30378
Surrogate: Dibromofluoromethane 103 Limits: 70-130%03/01/23 03:421 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%03/01/23 03:421 MSA V30378
Surrogate: Toluene-d8 106 Limits: 70-130%03/01/23 03:421 MSA V30378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 87 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-18
89762 Matrix:
2/23/2023 10:44
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 03/01/23 06:09 6200BMSA
Surrogate: 4-Bromofluorobenzene 92.4 Limits: 70-130%03/01/23 06:091 MSA V30378
Surrogate: Dibromofluoromethane 97.4 Limits: 70-130%03/01/23 06:091 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 108 Limits: 70-130%03/01/23 06:091 MSA V30378
Surrogate: Toluene-d8 102 Limits: 70-130%03/01/23 06:091 MSA V30378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 88 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-18
89762 Matrix:
2/23/2023 10:44
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 03/01/23 06:09 V30378MSA
<0.180 µg/L 0.180 0.500Benzene 1 03/01/23 06:09 V30378MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 03/01/23 06:09 V30378MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 03/01/23 06:09 V30378MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 03/01/23 06:09 V30378MSA
<1.50 µg/L 1.50 5.00Bromoform 1 03/01/23 06:09 V30378MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 03/01/23 06:09 V30378MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 03/01/23 06:09 V30378MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 03/01/23 06:09 V30378MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 03/01/23 06:09 V30378MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 03/01/23 06:09 V30378MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 03/01/23 06:09 V30378MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 03/01/23 06:09 V30378MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 03/01/23 06:09 V30378MSA
<0.220 µg/L 0.220 0.500Chloroform 1 03/01/23 06:09 V30378MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 03/01/23 06:09 V30378MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 03/01/23 06:09 V30378MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 03/01/23 06:09 V30378MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 03/01/23 06:09 V30378MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 03/01/23 06:09 V30378MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 03/01/23 06:09 V30378MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 03/01/23 06:09 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 89 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-18
89762 Matrix:
2/23/2023 10:44
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 03/01/23 06:09 V30378MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 03/01/23 06:09 V30378MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 03/01/23 06:09 V30378MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 03/01/23 06:09 V30378MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 03/01/23 06:09 V30378MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 03/01/23 06:09 V30378MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 03/01/23 06:09 V30378MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 03/01/23 06:09 V30378MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 03/01/23 06:09 V30378MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 03/01/23 06:09 V30378MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 03/01/23 06:09 V30378MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 03/01/23 06:09 V30378MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 03/01/23 06:09 V30378MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 03/01/23 06:09 V30378MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 03/01/23 06:09 V30378MSA
<42.0 µg/L 42.0 200
Ethanol 1 03/01/23 06:09 V30378MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 03/01/23 06:09 V30378MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 03/01/23 06:09 V30378MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 03/01/23 06:09 V30378MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 03/01/23 06:09 V30378MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 03/01/23 06:09 V30378MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 03/01/23 06:09 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 90 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-18
89762 Matrix:
2/23/2023 10:44
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 03/01/23 06:09 V30378MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 03/01/23 06:09 V30378MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 03/01/23 06:09 V30378MSA
2.77 µg/L 0.470 1.00Naphthalene 1 03/01/23 06:09 V30378MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 03/01/23 06:09 V30378MSA
<0.220 µg/L 0.220 0.500Styrene 1 03/01/23 06:09 V30378MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 03/01/23 06:09 V30378MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 03/01/23 06:09 V30378MSA
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 03/01/23 06:09 V30378MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 03/01/23 06:09 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 03/01/23 06:09 V30378MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 03/01/23 06:09 V30378MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 03/01/23 06:09 V30378MSA
<0.220 µg/L 0.220 0.500Toluene 1 03/01/23 06:09 V30378MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 03/01/23 06:09 V30378MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 03/01/23 06:09 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 03/01/23 06:09 V30378MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 03/01/23 06:09 V30378MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 03/01/23 06:09 V30378MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 03/01/23 06:09 V30378MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 03/01/23 06:09 V30378MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 03/01/23 06:09 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 91 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-18
89762 Matrix:
2/23/2023 10:44
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 03/01/23 06:09 V30378MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 03/01/23 06:09 V30378MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 03/01/23 06:09 V30378MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 03/01/23 06:09 V30378MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 03/01/23 06:09 V30378MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 03/01/23 06:09 V30378
Surrogate: 4-Bromofluorobenzene 92.4 Limits: 70-130%03/01/23 06:091 MSA V30378
Surrogate: Dibromofluoromethane 97.4 Limits: 70-130%03/01/23 06:091 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 108 Limits: 70-130%03/01/23 06:091 MSA V30378
Surrogate: Toluene-d8 102 Limits: 70-130%03/01/23 06:091 MSA V30378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 92 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-19
89763 Matrix:
2/23/2023 10:30
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 03/01/23 04:07 6200BMSA
Surrogate: 4-Bromofluorobenzene 93.8 Limits: 70-130%03/01/23 04:071 MSA V30378
Surrogate: Dibromofluoromethane 98.2 Limits: 70-130%03/01/23 04:071 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%03/01/23 04:071 MSA V30378
Surrogate: Toluene-d8 107 Limits: 70-130%03/01/23 04:071 MSA V30378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 93 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-19
89763 Matrix:
2/23/2023 10:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 03/01/23 04:07 V30378MSA
<0.180 µg/L 0.180 0.500Benzene 1 03/01/23 04:07 V30378MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 03/01/23 04:07 V30378MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 03/01/23 04:07 V30378MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 03/01/23 04:07 V30378MSA
<1.50 µg/L 1.50 5.00Bromoform 1 03/01/23 04:07 V30378MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 03/01/23 04:07 V30378MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 03/01/23 04:07 V30378MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 03/01/23 04:07 V30378MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 03/01/23 04:07 V30378MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 03/01/23 04:07 V30378MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 03/01/23 04:07 V30378MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 03/01/23 04:07 V30378MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 03/01/23 04:07 V30378MSA
<0.220 µg/L 0.220 0.500Chloroform 1 03/01/23 04:07 V30378MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 03/01/23 04:07 V30378MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 03/01/23 04:07 V30378MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 03/01/23 04:07 V30378MSA
2.01 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 03/01/23 04:07 V30378MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 03/01/23 04:07 V30378MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 03/01/23 04:07 V30378MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 03/01/23 04:07 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 94 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-19
89763 Matrix:
2/23/2023 10:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 03/01/23 04:07 V30378MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 03/01/23 04:07 V30378MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 03/01/23 04:07 V30378MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 03/01/23 04:07 V30378MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 03/01/23 04:07 V30378MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 03/01/23 04:07 V30378MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 03/01/23 04:07 V30378MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 03/01/23 04:07 V30378MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 03/01/23 04:07 V30378MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 03/01/23 04:07 V30378MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 03/01/23 04:07 V30378MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 03/01/23 04:07 V30378MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 03/01/23 04:07 V30378MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 03/01/23 04:07 V30378MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 03/01/23 04:07 V30378MSA
<42.0 µg/L 42.0 200
Ethanol 1 03/01/23 04:07 V30378MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 03/01/23 04:07 V30378MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 03/01/23 04:07 V30378MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 03/01/23 04:07 V30378MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 03/01/23 04:07 V30378MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 03/01/23 04:07 V30378MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 03/01/23 04:07 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 95 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-19
89763 Matrix:
2/23/2023 10:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 03/01/23 04:07 V30378MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 03/01/23 04:07 V30378MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 03/01/23 04:07 V30378MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 03/01/23 04:07 V30378MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 03/01/23 04:07 V30378MSA
<0.220 µg/L 0.220 0.500Styrene 1 03/01/23 04:07 V30378MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 03/01/23 04:07 V30378MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 03/01/23 04:07 V30378MSA
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 03/01/23 04:07 V30378MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 03/01/23 04:07 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 03/01/23 04:07 V30378MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 03/01/23 04:07 V30378MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 03/01/23 04:07 V30378MSA
<0.220 µg/L 0.220 0.500Toluene 1 03/01/23 04:07 V30378MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 03/01/23 04:07 V30378MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 03/01/23 04:07 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 03/01/23 04:07 V30378MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 03/01/23 04:07 V30378MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 03/01/23 04:07 V30378MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 03/01/23 04:07 V30378MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 03/01/23 04:07 V30378MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 03/01/23 04:07 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 96 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:MW-19
89763 Matrix:
2/23/2023 10:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 03/01/23 04:07 V30378MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 03/01/23 04:07 V30378MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 03/01/23 04:07 V30378MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 03/01/23 04:07 V30378MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 03/01/23 04:07 V30378MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 03/01/23 04:07 V30378
Surrogate: 4-Bromofluorobenzene 93.8 Limits: 70-130%03/01/23 04:071 MSA V30378
Surrogate: Dibromofluoromethane 98.2 Limits: 70-130%03/01/23 04:071 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%03/01/23 04:071 MSA V30378
Surrogate: Toluene-d8 107 Limits: 70-130%03/01/23 04:071 MSA V30378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 97 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:TW-1
89764 Matrix:
2/23/2023 15:03
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 03/01/23 04:31 6200BMSA
Surrogate: 4-Bromofluorobenzene 95.4 Limits: 70-130%03/01/23 04:311 MSA V30378
Surrogate: Dibromofluoromethane 99.8 Limits: 70-130%03/01/23 04:311 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 108 Limits: 70-130%03/01/23 04:311 MSA V30378
Surrogate: Toluene-d8 109 Limits: 70-130%03/01/23 04:311 MSA V30378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 98 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:TW-1
89764 Matrix:
2/23/2023 15:03
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 03/01/23 04:31 V30378MSA
1.85 µg/L 0.180 0.500Benzene 1 03/01/23 04:31 V30378MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 03/01/23 04:31 V30378MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 03/01/23 04:31 V30378MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 03/01/23 04:31 V30378MSA
<1.50 µg/L 1.50 5.00Bromoform 1 03/01/23 04:31 V30378MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 03/01/23 04:31 V30378MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 03/01/23 04:31 V30378MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 03/01/23 04:31 V30378MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 03/01/23 04:31 V30378MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 03/01/23 04:31 V30378MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 03/01/23 04:31 V30378MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 03/01/23 04:31 V30378MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 03/01/23 04:31 V30378MSA
1.45 µg/L 0.220 0.500Chloroform 1 03/01/23 04:31 V30378MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 03/01/23 04:31 V30378MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 03/01/23 04:31 V30378MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 03/01/23 04:31 V30378MSA
6.74 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 03/01/23 04:31 V30378MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 03/01/23 04:31 V30378MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 03/01/23 04:31 V30378MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 03/01/23 04:31 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 99 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:TW-1
89764 Matrix:
2/23/2023 15:03
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 03/01/23 04:31 V30378MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 03/01/23 04:31 V30378MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 03/01/23 04:31 V30378MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 03/01/23 04:31 V30378MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 03/01/23 04:31 V30378MSA
0.303 J µg/L 0.150 0.5001,2-Dichloroethane 1 03/01/23 04:31 V30378MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 03/01/23 04:31 V30378MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 03/01/23 04:31 V30378MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 03/01/23 04:31 V30378MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 03/01/23 04:31 V30378MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 03/01/23 04:31 V30378MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 03/01/23 04:31 V30378MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 03/01/23 04:31 V30378MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 03/01/23 04:31 V30378MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 03/01/23 04:31 V30378MSA
<42.0 µg/L 42.0 200
Ethanol 1 03/01/23 04:31 V30378MSA
0.460 J µg/L 0.170 0.500Ethylbenzene 1 03/01/23 04:31 V30378MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 03/01/23 04:31 V30378MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 03/01/23 04:31 V30378MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 03/01/23 04:31 V30378MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 03/01/23 04:31 V30378MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 03/01/23 04:31 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 100 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:TW-1
89764 Matrix:
2/23/2023 15:03
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 03/01/23 04:31 V30378MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 03/01/23 04:31 V30378MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 03/01/23 04:31 V30378MSA
1.24 µg/L 0.470 1.00Naphthalene 1 03/01/23 04:31 V30378MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 03/01/23 04:31 V30378MSA
<0.220 µg/L 0.220 0.500Styrene 1 03/01/23 04:31 V30378MSA
135 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 03/01/23 04:31 V30378MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 03/01/23 04:31 V30378MSA
41.2 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 03/01/23 04:31 V30378MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 03/01/23 04:31 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 03/01/23 04:31 V30378MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 03/01/23 04:31 V30378MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 03/01/23 04:31 V30378MSA
<0.220 µg/L 0.220 0.500Toluene 1 03/01/23 04:31 V30378MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 03/01/23 04:31 V30378MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 03/01/23 04:31 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 03/01/23 04:31 V30378MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 03/01/23 04:31 V30378MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 03/01/23 04:31 V30378MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 03/01/23 04:31 V30378MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 03/01/23 04:31 V30378MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 03/01/23 04:31 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 101 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:TW-1
89764 Matrix:
2/23/2023 15:03
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 03/01/23 04:31 V30378MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 03/01/23 04:31 V30378MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 03/01/23 04:31 V30378MSA
0.501 µg/L 0.210 0.500o-Xylene 1 03/01/23 04:31 V30378MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 03/01/23 04:31 V30378MSA
0.501 µg/L 0.210 0.500Xylene (Total)1 03/01/23 04:31 V30378
Surrogate: 4-Bromofluorobenzene 95.4 Limits: 70-130%03/01/23 04:311 MSA V30378
Surrogate: Dibromofluoromethane 99.8 Limits: 70-130%03/01/23 04:311 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 108 Limits: 70-130%03/01/23 04:311 MSA V30378
Surrogate: Toluene-d8 109 Limits: 70-130%03/01/23 04:311 MSA V30378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 102 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:RW-1
89765 Matrix:
2/23/2023 14:20
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 03/01/23 07:47 6200BMSA
Surrogate: 4-Bromofluorobenzene 96.4 Limits: 70-130%03/01/23 07:47100 MSA V30378
Surrogate: Dibromofluoromethane 96.0 Limits: 70-130%03/01/23 07:47100 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 109 Limits: 70-130%03/01/23 07:47100 MSA V30378
Surrogate: Toluene-d8 96.0 Limits: 70-130%03/01/23 07:47100 MSA V30378
Surrogate: 4-Bromofluorobenzene 95.8 Limits: 70-130%03/01/23 08:111000 MSA V30378
Surrogate: Dibromofluoromethane 99.6 Limits: 70-130%03/01/23 08:111000 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%03/01/23 08:111000 MSA V30378
Surrogate: Toluene-d8 104 Limits: 70-130%03/01/23 08:111000 MSA V30378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 103 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:RW-1
89765 Matrix:
2/23/2023 14:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<180 µg/L 180 1000Acetone 100 03/01/23 07:47 V30378MSA
6800 µg/L 18.0 50.0Benzene 100 03/01/23 07:47 V30378MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 03/01/23 07:47 V30378MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 03/01/23 07:47 V30378MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 03/01/23 07:47 V30378MSA
<150 µg/L 150 500Bromoform 100 03/01/23 07:47 V30378MSA
<28.0 µg/L 28.0 100Bromomethane 100 03/01/23 07:47 V30378MSA
37.1 J µg/L 18.0 50.0n-Butylbenzene 100 03/01/23 07:47 V30378MSA
<20.0 µg/L 20.0 50.0
sec-Butyl benzene 100 03/01/23 07:47 V30378MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 03/01/23 07:47 V30378MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 03/01/23 07:47 V30378MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 03/01/23 07:47 V30378MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 03/01/23 07:47 V30378MSA
<43.0 µg/L 43.0 100Chloroethane 100 03/01/23 07:47 V30378MSA
<22.0 µg/L 22.0 50.0Chloroform 100 03/01/23 07:47 V30378MSA
<22.0 µg/L 22.0 50.0
Chloromethane 100 03/01/23 07:47 V30378MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 03/01/23 07:47 V30378MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 03/01/23 07:47 V30378MSA
191 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 03/01/23 07:47 V30378MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 03/01/23 07:47 V30378MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 03/01/23 07:47 V30378MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 03/01/23 07:47 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 104 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:RW-1
89765 Matrix:
2/23/2023 14:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 03/01/23 07:47 V30378MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 03/01/23 07:47 V30378MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 03/01/23 07:47 V30378MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 03/01/23 07:47 V30378MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 03/01/23 07:47 V30378MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 03/01/23 07:47 V30378MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 03/01/23 07:47 V30378MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 03/01/23 07:47 V30378MSA
<18.0 µg/L 18.0 50.0
trans-1,2-Dichloroethene 100 03/01/23 07:47 V30378MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 03/01/23 07:47 V30378MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 03/01/23 07:47 V30378MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 03/01/23 07:47 V30378MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 03/01/23 07:47 V30378MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 03/01/23 07:47 V30378MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 03/01/23 07:47 V30378MSA
<4200 µg/L 4200 20000
Ethanol 100 03/01/23 07:47 V30378MSA
2380 µg/L 17.0 50.0Ethylbenzene 100 03/01/23 07:47 V30378MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 03/01/23 07:47 V30378MSA
<38.0 µg/L 38.0 1002-Hexanone 100 03/01/23 07:47 V30378MSA
81.5 µg/L 18.0 50.0Isopropylbenzene 100 03/01/23 07:47 V30378MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 03/01/23 07:47 V30378MSA
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 03/01/23 07:47 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 105 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:RW-1
89765 Matrix:
2/23/2023 14:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<14.0 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 03/01/23 07:47 V30378MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 03/01/23 07:47 V30378MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 03/01/23 07:47 V30378MSA
929 µg/L 47.0 100Naphthalene 100 03/01/23 07:47 V30378MSA
252 µg/L 19.0 50.0n-Propylbenzene 100 03/01/23 07:47 V30378MSA
109 µg/L 22.0 50.0Styrene 100 03/01/23 07:47 V30378MSA
<160 µg/L 160 1000tert-Butyl Alcohol (TBA)100 03/01/23 07:47 V30378MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 03/01/23 07:47 V30378MSA
1970 µg/L 190 1000
tert-Amyl Alcohol (TAA)100 03/01/23 07:47 V30378MSA
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 03/01/23 07:47 V30378MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 03/01/23 07:47 V30378MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 03/01/23 07:47 V30378MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 03/01/23 07:47 V30378MSA
25400 µg/L 220 500Toluene 1000 03/01/23 08:11 V30378MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 03/01/23 07:47 V30378MSA
<31.0 µg/L 31.0 50.0
1,2,4-Trichlorobenzene 100 03/01/23 07:47 V30378MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 03/01/23 07:47 V30378MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 03/01/23 07:47 V30378MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 03/01/23 07:47 V30378MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 03/01/23 07:47 V30378MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 03/01/23 07:47 V30378MSA
2220 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 03/01/23 07:47 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 106 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:RW-1
89765 Matrix:
2/23/2023 14:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
634 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 03/01/23 07:47 V30378MSA
<100 µg/L 100 500Vinyl Acetate 100 03/01/23 07:47 V30378MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 03/01/23 07:47 V30378MSA
4090 µg/L 21.0 50.0o-Xylene 100 03/01/23 07:47 V30378MSA
10300 µg/L 42.0 100m,p-Xylene 100 03/01/23 07:47 V30378MSA
14400 µg/L 21.0 50.0Xylene (Total)100 03/01/23 07:47 V30378
Surrogate: 4-Bromofluorobenzene 96.4 Limits: 70-130%03/01/23 07:47100 MSA V30378
Surrogate: Dibromofluoromethane 96.0 Limits: 70-130%03/01/23 07:47100 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 109 Limits: 70-130%03/01/23 07:47100 MSA V30378
Surrogate: Toluene-d8 96.0 Limits: 70-130%03/01/23 07:47100 MSA V30378
Surrogate: 4-Bromofluorobenzene 95.8 Limits: 70-130%03/01/23 08:111000 MSA V30378
Surrogate: Dibromofluoromethane 99.6 Limits: 70-130%03/01/23 08:111000 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%03/01/23 08:111000 MSA V30378
Surrogate: Toluene-d8 104 Limits: 70-130%03/01/23 08:111000 MSA V30378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 107 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:RW-2
89766 Matrix:
2/23/2023 14:33
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 03/01/23 06:34 6200BMSA
Surrogate: 4-Bromofluorobenzene 81.8 Limits: 70-130%03/01/23 06:341 MSA V30378
Surrogate: Dibromofluoromethane 95.6 Limits: 70-130%03/01/23 06:341 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%03/01/23 06:341 MSA V30378
Surrogate: Toluene-d8 104 Limits: 70-130%03/01/23 06:341 MSA V30378
Surrogate: 4-Bromofluorobenzene 99.8 Limits: 70-130%03/02/23 01:3410 MSA V30431
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%03/02/23 01:3410 MSA V30431
Surrogate: 1,2-Dichloroethane - d4 95.4 Limits: 70-130%03/02/23 01:3410 MSA V30431
Surrogate: Toluene-d8 99.8 Limits: 70-130%03/02/23 01:3410 MSA V30431
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 108 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:RW-2
89766 Matrix:
2/23/2023 14:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00 V30429 03/01/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 03/01/23 06:34 V30378MSA
6.51 µg/L 0.180 0.500Benzene 1 03/01/23 06:34 V30378MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 03/01/23 06:34 V30378MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 03/01/23 06:34 V30378MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 03/01/23 06:34 V30378MSA
<1.50 µg/L 1.50 5.00Bromoform 1 03/01/23 06:34 V30378MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 03/01/23 06:34 V30378MSA
0.769 µg/L 0.180 0.500n-Butylbenzene 1 03/01/23 06:34 V30378MSA
0.542 µg/L 0.200 0.500
sec-Butyl benzene 1 03/01/23 06:34 V30378MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 03/01/23 06:34 V30378MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 03/01/23 06:34 V30378MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 03/01/23 06:34 V30378MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 03/01/23 06:34 V30378MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 03/01/23 06:34 V30378MSA
5.47 µg/L 0.220 0.500Chloroform 1 03/01/23 06:34 V30378MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 03/01/23 06:34 V30378MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 03/01/23 06:34 V30378MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 03/01/23 06:34 V30378MSA
14.0 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 03/01/23 06:34 V30378MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 03/01/23 06:34 V30378MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 03/01/23 06:34 V30378MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 03/01/23 06:34 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 109 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:RW-2
89766 Matrix:
2/23/2023 14:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00 V30429 03/01/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 03/01/23 06:34 V30378MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 03/01/23 06:34 V30378MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 03/01/23 06:34 V30378MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 03/01/23 06:34 V30378MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 03/01/23 06:34 V30378MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 03/01/23 06:34 V30378MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 03/01/23 06:34 V30378MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 03/01/23 06:34 V30378MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 03/01/23 06:34 V30378MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 03/01/23 06:34 V30378MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 03/01/23 06:34 V30378MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 03/01/23 06:34 V30378MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 03/01/23 06:34 V30378MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 03/01/23 06:34 V30378MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 03/01/23 06:34 V30378MSA
<42.0 µg/L 42.0 200
Ethanol 1 03/01/23 06:34 V30378MSA
17.0 µg/L 0.170 0.500Ethylbenzene 1 03/01/23 06:34 V30378MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 03/01/23 06:34 V30378MSA
9.86 µg/L 0.380 1.002-Hexanone 1 03/01/23 06:34 V30378MSA
1.24 µg/L 0.180 0.500Isopropylbenzene 1 03/01/23 06:34 V30378MSA
0.508 µg/L 0.089 0.5004-Isopropyl toluene 1 03/01/23 06:34 V30378MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 03/01/23 06:34 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 110 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:RW-2
89766 Matrix:
2/23/2023 14:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00 V30429 03/01/23 09:00
90.4 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 03/01/23 06:34 V30378MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 03/01/23 06:34 V30378MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 03/01/23 06:34 V30378MSA
12.1 µg/L 0.470 1.00Naphthalene 1 03/01/23 06:34 V30378MSA
2.76 µg/L 0.190 0.500n-Propylbenzene 1 03/01/23 06:34 V30378MSA
<0.220 µg/L 0.220 0.500Styrene 1 03/01/23 06:34 V30378MSA
237 µg/L 16.0 100tert-Butyl Alcohol (TBA)10 03/02/23 01:34 V30431MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 03/01/23 06:34 V30378MSA
187 µg/L 19.0 100
tert-Amyl Alcohol (TAA)10 03/02/23 01:34 V30431MSA
3.55 J µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 03/01/23 06:34 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 03/01/23 06:34 V30378MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 03/01/23 06:34 V30378MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 03/01/23 06:34 V30378MSA
64.4 µg/L 0.220 0.500Toluene 1 03/01/23 06:34 V30378MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 03/01/23 06:34 V30378MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 03/01/23 06:34 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 03/01/23 06:34 V30378MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 03/01/23 06:34 V30378MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 03/01/23 06:34 V30378MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 03/01/23 06:34 V30378MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 03/01/23 06:34 V30378MSA
59.1 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 03/01/23 06:34 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 111 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:RW-2
89766 Matrix:
2/23/2023 14:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00 V30429 03/01/23 09:00
19.1 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 03/01/23 06:34 V30378MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 03/01/23 06:34 V30378MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 03/01/23 06:34 V30378MSA
67.4 µg/L 0.210 0.500o-Xylene 1 03/01/23 06:34 V30378MSA
169 µg/L 0.420 1.00m,p-Xylene 1 03/01/23 06:34 V30378MSA
236 µg/L 0.210 0.500Xylene (Total)1 03/01/23 06:34 V30378
Surrogate: 4-Bromofluorobenzene 81.8 Limits: 70-130%03/01/23 06:341 MSA V30378
Surrogate: Dibromofluoromethane 95.6 Limits: 70-130%03/01/23 06:341 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%03/01/23 06:341 MSA V30378
Surrogate: Toluene-d8 104 Limits: 70-130%03/01/23 06:341 MSA V30378
Surrogate: 4-Bromofluorobenzene 99.8 Limits: 70-130%03/02/23 01:3410 MSA V30431
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%03/02/23 01:3410 MSA V30431
Surrogate: 1,2-Dichloroethane - d4 95.4 Limits: 70-130%03/02/23 01:3410 MSA V30431
Surrogate: Toluene-d8 99.8 Limits: 70-130%03/02/23 01:3410 MSA V30431
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 112 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:RW-3
89767 Matrix:
2/23/2023 14:42
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 03/01/23 04:56 6200BMSA
Surrogate: 4-Bromofluorobenzene 108 Limits: 70-130%03/01/23 04:561 MSA V30378
Surrogate: Dibromofluoromethane 88.0 Limits: 70-130%03/01/23 04:561 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 117 Limits: 70-130%03/01/23 04:561 MSA V30378
Surrogate: Toluene-d8 99.2 Limits: 70-130%03/01/23 04:561 MSA V30378
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%03/02/23 02:47100 MSA V30431
Surrogate: Dibromofluoromethane 101 Limits: 70-130%03/02/23 02:47100 MSA V30431
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%03/02/23 02:47100 MSA V30431
Surrogate: Toluene-d8 99.8 Limits: 70-130%03/02/23 02:47100 MSA V30431
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 113 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:RW-3
89767 Matrix:
2/23/2023 14:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00 V30429 03/01/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 03/01/23 04:56 V30378MSA
1030 µg/L 18.0 50.0Benzene 100 03/02/23 02:47 V30431MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 03/01/23 04:56 V30378MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 03/01/23 04:56 V30378MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 03/01/23 04:56 V30378MSA
<1.50 µg/L 1.50 5.00Bromoform 1 03/01/23 04:56 V30378MSA
4.61 µg/L 0.280 1.00Bromomethane 1 03/01/23 04:56 V30378MSA
9.87 µg/L 0.180 0.500n-Butylbenzene 1 03/01/23 04:56 V30378MSA
4.37 µg/L 0.200 0.500
sec-Butyl benzene 1 03/01/23 04:56 V30378MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 03/01/23 04:56 V30378MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 03/01/23 04:56 V30378MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 03/01/23 04:56 V30378MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 03/01/23 04:56 V30378MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 03/01/23 04:56 V30378MSA
<0.220 µg/L 0.220 0.500Chloroform 1 03/01/23 04:56 V30378MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 03/01/23 04:56 V30378MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 03/01/23 04:56 V30378MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 03/01/23 04:56 V30378MSA
63.9 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 03/01/23 04:56 V30378MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 03/01/23 04:56 V30378MSA
16.5 µg/L 0.200 0.5001,2-Dibromoethane 1 03/01/23 04:56 V30378MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 03/01/23 04:56 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 114 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:RW-3
89767 Matrix:
2/23/2023 14:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00 V30429 03/01/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 03/01/23 04:56 V30378MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 03/01/23 04:56 V30378MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 03/01/23 04:56 V30378MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 03/01/23 04:56 V30378MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 03/01/23 04:56 V30378MSA
14.9 µg/L 0.150 0.5001,2-Dichloroethane 1 03/01/23 04:56 V30378MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 03/01/23 04:56 V30378MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 03/01/23 04:56 V30378MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 03/01/23 04:56 V30378MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 03/01/23 04:56 V30378MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 03/01/23 04:56 V30378MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 03/01/23 04:56 V30378MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 03/01/23 04:56 V30378MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 03/01/23 04:56 V30378MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 03/01/23 04:56 V30378MSA
<42.0 µg/L 42.0 200
Ethanol 1 03/01/23 04:56 V30378MSA
564 µg/L 17.0 50.0Ethylbenzene 100 03/02/23 02:47 V30431MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 03/01/23 04:56 V30378MSA
31.5 µg/L 0.380 1.002-Hexanone 1 03/01/23 04:56 V30378MSA
28.9 µg/L 0.180 0.500Isopropylbenzene 1 03/01/23 04:56 V30378MSA
2.82 µg/L 0.089 0.5004-Isopropyl toluene 1 03/01/23 04:56 V30378MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 03/01/23 04:56 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 115 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:RW-3
89767 Matrix:
2/23/2023 14:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00 V30429 03/01/23 09:00
91.8 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 03/01/23 04:56 V30378MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 03/01/23 04:56 V30378MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 03/01/23 04:56 V30378MSA
211 µg/L 47.0 100Naphthalene 100 03/02/23 02:47 V30431MSA
86.0 µg/L 0.190 0.500n-Propylbenzene 1 03/01/23 04:56 V30378MSA
24.3 µg/L 0.220 0.500Styrene 1 03/01/23 04:56 V30378MSA
608 J µg/L 160 1000tert-Butyl Alcohol (TBA)100 03/02/23 02:47 V30431MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 03/01/23 04:56 V30378MSA
635 µg/L 190 1000
tert-Amyl Alcohol (TAA)100 03/02/23 02:47 V30431MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 03/01/23 04:56 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 03/01/23 04:56 V30378MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 03/01/23 04:56 V30378MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 03/01/23 04:56 V30378MSA
3110 µg/L 22.0 50.0Toluene 100 03/02/23 02:47 V30431MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 03/01/23 04:56 V30378MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 03/01/23 04:56 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 03/01/23 04:56 V30378MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 03/01/23 04:56 V30378MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 03/01/23 04:56 V30378MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 03/01/23 04:56 V30378MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 03/01/23 04:56 V30378MSA
621 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 03/02/23 02:47 V30431MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 116 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:RW-3
89767 Matrix:
2/23/2023 14:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00 V30429 03/01/23 09:00
155 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 03/02/23 02:47 V30431MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 03/01/23 04:56 V30378MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 03/01/23 04:56 V30378MSA
797 µg/L 21.0 50.0o-Xylene 100 03/02/23 02:47 V30431MSA
1940 µg/L 42.0 100m,p-Xylene 100 03/02/23 02:47 V30431MSA
2740 µg/L 21.0 50.0Xylene (Total)100 03/02/23 02:47 V30431
Surrogate: 4-Bromofluorobenzene 108 Limits: 70-130%03/01/23 04:561 MSA V30378
Surrogate: Dibromofluoromethane 88.0 Limits: 70-130%03/01/23 04:561 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 117 Limits: 70-130%03/01/23 04:561 MSA V30378
Surrogate: Toluene-d8 99.2 Limits: 70-130%03/01/23 04:561 MSA V30378
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%03/02/23 02:47100 MSA V30431
Surrogate: Dibromofluoromethane 101 Limits: 70-130%03/02/23 02:47100 MSA V30431
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%03/02/23 02:47100 MSA V30431
Surrogate: Toluene-d8 99.8 Limits: 70-130%03/02/23 02:47100 MSA V30431
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 117 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:Trip Blank
89768 Matrix:
2/23/2023 9:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 03/01/23 02:05 V30378MSA
<0.180 µg/L 0.180 0.500Benzene 1 03/01/23 02:05 V30378MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 03/01/23 02:05 V30378MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 03/01/23 02:05 V30378MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 03/01/23 02:05 V30378MSA
<1.50 µg/L 1.50 5.00Bromoform 1 03/01/23 02:05 V30378MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 03/01/23 02:05 V30378MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 03/01/23 02:05 V30378MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 03/01/23 02:05 V30378MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 03/01/23 02:05 V30378MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 03/01/23 02:05 V30378MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 03/01/23 02:05 V30378MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 03/01/23 02:05 V30378MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 03/01/23 02:05 V30378MSA
<0.220 µg/L 0.220 0.500Chloroform 1 03/01/23 02:05 V30378MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 03/01/23 02:05 V30378MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 03/01/23 02:05 V30378MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 03/01/23 02:05 V30378MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 03/01/23 02:05 V30378MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 03/01/23 02:05 V30378MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 03/01/23 02:05 V30378MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 03/01/23 02:05 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 118 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:Trip Blank
89768 Matrix:
2/23/2023 9:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 03/01/23 02:05 V30378MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 03/01/23 02:05 V30378MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 03/01/23 02:05 V30378MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 03/01/23 02:05 V30378MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 03/01/23 02:05 V30378MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 03/01/23 02:05 V30378MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 03/01/23 02:05 V30378MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 03/01/23 02:05 V30378MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 03/01/23 02:05 V30378MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 03/01/23 02:05 V30378MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 03/01/23 02:05 V30378MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 03/01/23 02:05 V30378MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 03/01/23 02:05 V30378MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 03/01/23 02:05 V30378MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 03/01/23 02:05 V30378MSA
<42.0 µg/L 42.0 200
Ethanol 1 03/01/23 02:05 V30378MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 03/01/23 02:05 V30378MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 03/01/23 02:05 V30378MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 03/01/23 02:05 V30378MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 03/01/23 02:05 V30378MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 03/01/23 02:05 V30378MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 03/01/23 02:05 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 119 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:Trip Blank
89768 Matrix:
2/23/2023 9:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 03/01/23 02:05 V30378MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 03/01/23 02:05 V30378MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 03/01/23 02:05 V30378MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 03/01/23 02:05 V30378MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 03/01/23 02:05 V30378MSA
<0.220 µg/L 0.220 0.500Styrene 1 03/01/23 02:05 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 03/01/23 02:05 V30378MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 03/01/23 02:05 V30378MSA
<0.220 µg/L 0.220 0.500
Tetrachloroethene 1 03/01/23 02:05 V30378MSA
<0.220 µg/L 0.220 0.500Toluene 1 03/01/23 02:05 V30378MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 03/01/23 02:05 V30378MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 03/01/23 02:05 V30378MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 03/01/23 02:05 V30378MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 03/01/23 02:05 V30378MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 03/01/23 02:05 V30378MSA
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 03/01/23 02:05 V30378MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 03/01/23 02:05 V30378MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 03/01/23 02:05 V30378MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 03/01/23 02:05 V30378MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 03/01/23 02:05 V30378MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 03/01/23 02:05 V30378MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 03/01/23 02:05 V30378MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 120 of 140
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-055-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 02/24/2023
Kingsway #10
Report Date : 03/08/2023
Sample ID :
Lab No :
Sampled:Trip Blank
89768 Matrix:
2/23/2023 9:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30377 02/28/23 14:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 03/01/23 02:05 V30378MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 03/01/23 02:05 V30378
Surrogate: 4-Bromofluorobenzene 91.2 Limits: 70-130%03/01/23 02:051 MSA V30378
Surrogate: Dibromofluoromethane 100 Limits: 70-130%03/01/23 02:051 MSA V30378
Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%03/01/23 02:051 MSA V30378
Surrogate: Toluene-d8 105 Limits: 70-130%03/01/23 02:051 MSA V30378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 121 of 140
Quality Control Data
23-055-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30280QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30279
Associated Lab Samples: 89747, 89748, 89749, 89750, 89751, 89752, 89753, 89754, 89755, 89756
LRB-V30279 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/28/23 14:1810.01.80<1.80µg/LAcetone
02/28/23 14:180.5000.180<0.180µg/LBenzene
02/28/23 14:180.5000.210<0.210µg/LBromobenzene
02/28/23 14:181.000.420<0.420µg/LBromochloromethane
02/28/23 14:180.5000.160<0.160µg/LBromodichloromethane
02/28/23 14:185.001.50<1.50µg/LBromoform
02/28/23 14:181.000.280<0.280µg/LBromomethane
02/28/23 14:180.5000.180<0.180µg/Ln-Butylbenzene
02/28/23 14:180.5000.200<0.200µg/Lsec-Butyl benzene
02/28/23 14:182.000.920<0.920µg/Ltert-Butyl benzene
02/28/23 14:180.5000.180<0.180µg/LCarbon Tetrachloride
02/28/23 14:180.5000.190<0.190µg/LChlorobenzene
02/28/23 14:180.5000.190<0.190µg/LChlorodibromomethane
02/28/23 14:181.000.430<0.430µg/LChloroethane
02/28/23 14:180.5000.220<0.220µg/LChloroform
02/28/23 14:180.5000.220<0.220µg/LChloromethane
02/28/23 14:180.5000.200<0.200µg/L2-Chlorotoluene
02/28/23 14:180.5000.200<0.200µg/L4-Chlorotoluene
02/28/23 14:180.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
02/28/23 14:182.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
02/28/23 14:180.5000.200<0.200µg/L1,2-Dibromoethane
02/28/23 14:180.5000.230<0.230µg/LDibromomethane
02/28/23 14:180.5000.220<0.220µg/L1,2-Dichlorobenzene
02/28/23 14:180.5000.190<0.190µg/L1,3-Dichlorobenzene
02/28/23 14:180.5000.210<0.210µg/L1,4-Dichlorobenzene
02/28/23 14:185.001.20<1.20µg/LDichlorodifluoromethane
02/28/23 14:180.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 15Date:03/08/2023 02:20 PM
Page 122 of 140
Quality Control Data
23-055-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30280QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30279
Associated Lab Samples: 89747, 89748, 89749, 89750, 89751, 89752, 89753, 89754, 89755, 89756
LRB-V30279 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/28/23 14:180.5000.150<0.150µg/L1,2-Dichloroethane
02/28/23 14:180.5000.150<0.150µg/L1,1-Dichloroethene
02/28/23 14:180.5000.200<0.200µg/Lcis-1,2-Dichloroethene
02/28/23 14:180.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
02/28/23 14:180.5000.190<0.190µg/L1,2-Dichloropropane
02/28/23 14:180.5000.130<0.130µg/L1,3-Dichloropropane
02/28/23 14:182.000.210<0.210µg/L2,2-Dichloropropane
02/28/23 14:180.5000.200<0.200µg/L1,1-Dichloropropene
02/28/23 14:180.5000.210<0.210µg/Lcis-1,3-Dichloropropene
02/28/23 14:180.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
02/28/23 14:1820042.0<42.0µg/LEthanol
02/28/23 14:180.5000.170<0.170µg/LEthylbenzene
02/28/23 14:183.000.350<0.350µg/LHexachlorobutadiene
02/28/23 14:181.000.380<0.380µg/L2-Hexanone
02/28/23 14:180.5000.180<0.180µg/LIsopropylbenzene
02/28/23 14:180.5000.089<0.089µg/L4-Isopropyl toluene
02/28/23 14:185.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
02/28/23 14:181.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
02/28/23 14:181.000.078<0.078µg/L4-Methyl-2-Pentanone
02/28/23 14:182.000.330<0.330µg/LMethylene Chloride
02/28/23 14:181.000.470<0.470µg/LNaphthalene
02/28/23 14:180.5000.190<0.190µg/Ln-Propylbenzene
02/28/23 14:180.5000.220<0.220µg/LStyrene
02/28/23 14:1810.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
02/28/23 14:1810.00.350<0.350µg/Ltert-Butyl formate (TBF)
02/28/23 14:1810.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
02/28/23 14:1810.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 2 of 15Date:03/08/2023 02:20 PM
Page 123 of 140
Quality Control Data
23-055-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30280QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30279
Associated Lab Samples: 89747, 89748, 89749, 89750, 89751, 89752, 89753, 89754, 89755, 89756
LRB-V30279 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/28/23 14:180.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
02/28/23 14:180.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
02/28/23 14:180.5000.220<0.220µg/LTetrachloroethene
02/28/23 14:180.5000.220<0.220µg/LToluene
02/28/23 14:180.5000.380<0.380µg/L1,2,3-Trichlorobenzene
02/28/23 14:180.5000.310<0.310µg/L1,2,4-Trichlorobenzene
02/28/23 14:180.5000.160<0.160µg/L1,1,1-Trichloroethane
02/28/23 14:180.5000.096<0.096µg/L1,1,2-Trichloroethane
02/28/23 14:180.5000.180<0.180µg/LTrichloroethene
02/28/23 14:180.5000.180<0.180µg/LTrichlorofluoromethane
02/28/23 14:180.5000.270<0.270µg/L1,2,3-Trichloropropane
02/28/23 14:180.5000.190<0.190µg/L1,2,4-Trimethylbenzene
02/28/23 14:180.5000.180<0.180µg/L1,3,5-Trimethylbenzene
02/28/23 14:185.001.00<1.00µg/LVinyl Acetate
02/28/23 14:180.5000.170<0.170µg/LVinyl Chloride
02/28/23 14:180.5000.210<0.210µg/Lo-Xylene
02/28/23 14:181.000.420<0.420µg/Lm,p-Xylene
02/28/23 14:1810.01.00<1.00µg/L3,3-Dimethyl-1-butanol
02/28/23 14:184-Bromofluorobenzene (S)95.8 70-130
02/28/23 14:18Dibromofluoromethane (S)103 70-130
02/28/23 14:181,2-Dichloroethane - d4 (S)108 70-130
02/28/23 14:18Toluene-d8 (S)104 70-130
Page 3 of 15Date:03/08/2023 02:20 PM
Page 124 of 140
Quality Control Data
23-055-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30280QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30279
LCS-V30279 LCSD-V30279Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
31.8 79.573.029.240.0µg/LAcetone 40-160 8.5 20.0
18.7 93.595.519.120.0µg/LBenzene 70-130 2.1 20.0
19.6 98.099.019.820.0µg/LBromobenzene 70-130 1.0 20.0
18.3 91.595.519.120.0µg/LBromochloromethane 70-130 4.2 20.0
21.3 10711022.020.0µg/LBromodichloromethane 70-130 3.2 20.0
21.3 10710320.620.0µg/LBromomethane 60-140 3.3 20.0
18.8 94.093.018.620.0µg/Ln-Butylbenzene 70-130 1.0 20.0
17.7 88.591.518.320.0µg/Lsec-Butyl benzene 70-130 3.3 20.0
17.4 87.088.517.720.0µg/Ltert-Butyl benzene 70-130 1.7 20.0
22.0 11010621.220.0µg/LCarbon Tetrachloride 70-130 3.7 20.0
19.3 96.599.019.820.0µg/LChlorobenzene 70-130 2.5 20.0
22.6 11310721.420.0µg/LChlorodibromomethane 70-130 5.4 20.0
21.0 10510320.520.0µg/LChloroethane 60-140 2.4 20.0
19.6 98.099.519.920.0µg/LChloroform 70-130 1.5 20.0
19.9 99.510320.620.0µg/LChloromethane 60-140 3.4 20.0
19.0 95.091.518.320.0µg/L2-Chlorotoluene 70-130 3.7 20.0
19.3 96.596.019.220.0µg/L4-Chlorotoluene 70-130 0.5 20.0
19.5 97.597.019.420.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.5 20.0
25.4 12711523.020.0µg/L1,2-Dibromo-3-Chloropropane 70-130 9.9 20.0
18.7 93.592.518.520.0µg/L1,2-Dibromoethane 70-130 1.0 20.0
21.3 10710320.620.0µg/LDibromomethane 70-130 3.3 20.0
19.2 96.091.518.320.0µg/L1,2-Dichlorobenzene 70-130 4.8 20.0
18.3 91.593.018.620.0µg/L1,3-Dichlorobenzene 70-130 1.6 20.0
18.6 93.091.018.220.0µg/L1,4-Dichlorobenzene 70-130 2.1 20.0
16.4 82.087.517.520.0µg/LDichlorodifluoromethane 60-140 6.4 20.0
18.0 90.096.019.220.0µg/L1,1-Dichloroethane 70-130 6.4 20.0
Page 4 of 15Date:03/08/2023 02:20 PM
Page 125 of 140
Quality Control Data
23-055-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30280QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30279
LCS-V30279 LCSD-V30279Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.9 11010921.820.0µg/L1,2-Dichloroethane 70-130 0.4 20.0
18.5 92.599.519.920.0µg/L1,1-Dichloroethene 70-130 7.2 20.0
18.7 93.597.519.520.0µg/Lcis-1,2-Dichloroethene 70-130 4.1 20.0
18.4 92.096.019.220.0µg/Ltrans-1,2-Dichloroethene 70-130 4.2 20.0
19.0 95.096.519.320.0µg/L1,2-Dichloropropane 70-130 1.5 20.0
19.9 99.594.018.820.0µg/L1,3-Dichloropropane 70-130 5.6 20.0
20.3 10210621.120.0µg/L2,2-Dichloropropane 70-130 3.8 20.0
18.8 94.094.018.820.0µg/L1,1-Dichloropropene 70-130 0.0 20.0
20.4 10210821.620.0µg/Lcis-1,3-Dichloropropene 70-130 5.7 20.0
23.5 11811623.220.0µg/Ltrans-1,3-Dichloropropene 70-130 1.2 20.0
597 11995.4477500µg/LEthanol 60-140 22.3*20.0
19.9 99.510220.320.0µg/LEthylbenzene 70-130 1.9 20.0
17.5 87.587.517.520.0µg/LHexachlorobutadiene 70-130 0.0 20.0
22.6 11310621.120.0µg/L2-Hexanone 60-140 6.8 20.0
17.6 88.086.017.220.0µg/LIsopropylbenzene 70-130 2.2 20.0
18.2 91.091.518.320.0µg/L4-Isopropyl toluene 70-130 0.5 20.0
19.1 95.592.018.420.0µg/LMethyl Ethyl Ketone (MEK)60-140 3.7 20.0
19.2 96.095.019.020.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.0 20.0
23.9 12011823.620.0µg/L4-Methyl-2-Pentanone 60-140 1.2 20.0
20.0 10095.519.120.0µg/LMethylene Chloride 70-130 4.6 20.0
19.3 96.585.517.120.0µg/LNaphthalene 70-130 12.0 20.0
17.6 88.087.017.420.0µg/Ln-Propylbenzene 70-130 1.1 20.0
18.5 92.591.518.320.0µg/LStyrene 70-130 1.0 20.0
51.1 12811646.340.0µg/Ltert-Butyl Alcohol (TBA)40-140 9.8 20.0
21.3 10710621.220.0µg/Ltert-Amyl Alcohol (TAA)40-140 0.4 20.0
41.9 10510441.640.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 0.7 20.0
Page 5 of 15* QC Fail Date:03/08/2023 02:20 PM
Page 126 of 140
Quality Control Data
23-055-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30280QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30279
LCS-V30279 LCSD-V30279Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
22.6 11311322.520.0µg/L1,1,1,2-Tetrachloroethane 70-130 0.4 20.0
22.2 11110320.520.0µg/L1,1,2,2-Tetrachloroethane 70-130 7.9 20.0
18.0 90.087.517.520.0µg/LTetrachloroethene 70-130 2.8 20.0
21.3 10711122.120.0µg/LToluene 70-130 3.6 20.0
19.9 99.593.518.720.0µg/L1,2,3-Trichlorobenzene 70-130 6.2 20.0
20.0 10091.518.320.0µg/L1,2,4-Trichlorobenzene 70-130 8.8 20.0
18.4 92.094.018.820.0µg/L1,1,1-Trichloroethane 70-130 2.1 20.0
21.3 10798.019.620.0µg/L1,1,2-Trichloroethane 70-130 8.3 20.0
17.3 86.591.018.220.0µg/LTrichloroethene 70-130 5.0 20.0
20.9 10510621.120.0µg/LTrichlorofluoromethane 60-140 0.9 20.0
19.8 99.092.518.520.0µg/L1,2,3-Trichloropropane 70-130 6.7 20.0
17.9 89.589.517.920.0µg/L1,2,4-Trimethylbenzene 70-130 0.0 20.0
19.2 96.095.019.020.0µg/L1,3,5-Trimethylbenzene 70-130 1.0 20.0
32.0 160*159*31.820.0µg/LVinyl Acetate 60-140 0.6 20.0
21.3 10711422.720.0µg/LVinyl Chloride 60-140 6.3 20.0
17.8 89.092.018.420.0µg/Lo-Xylene 70-130 3.3 20.0
41.8 10510642.340.0µg/Lm,p-Xylene 70-130 1.1 20.0
18.2 91.012024.020.0µg/L3,3-Dimethyl-1-butanol 70-130 27.4*20.0
94.693.24-Bromofluorobenzene (S)70-130
96.495.6Dibromofluoromethane (S)70-130
1131101,2-Dichloroethane - d4 (S)70-130
103102Toluene-d8 (S)70-130
Page 6 of 15* QC Fail Date:03/08/2023 02:20 PM
Page 127 of 140
Quality Control Data
23-055-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30378QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30377
Associated Lab Samples: 89757, 89758, 89759, 89760, 89761, 89762, 89763, 89764, 89765, 89766, 89767, 89768
LRB-V30377 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/01/23 01:4010.01.80<1.80µg/LAcetone
03/01/23 01:400.5000.180<0.180µg/LBenzene
03/01/23 01:400.5000.210<0.210µg/LBromobenzene
03/01/23 01:401.000.420<0.420µg/LBromochloromethane
03/01/23 01:400.5000.160<0.160µg/LBromodichloromethane
03/01/23 01:405.001.50<1.50µg/LBromoform
03/01/23 01:401.000.280<0.280µg/LBromomethane
03/01/23 01:400.5000.180<0.180µg/Ln-Butylbenzene
03/01/23 01:400.5000.200<0.200µg/Lsec-Butyl benzene
03/01/23 01:402.000.920<0.920µg/Ltert-Butyl benzene
03/01/23 01:400.5000.180<0.180µg/LCarbon Tetrachloride
03/01/23 01:400.5000.190<0.190µg/LChlorobenzene
03/01/23 01:400.5000.190<0.190µg/LChlorodibromomethane
03/01/23 01:401.000.430<0.430µg/LChloroethane
03/01/23 01:400.5000.220<0.220µg/LChloroform
03/01/23 01:400.5000.220<0.220µg/LChloromethane
03/01/23 01:400.5000.200<0.200µg/L2-Chlorotoluene
03/01/23 01:400.5000.200<0.200µg/L4-Chlorotoluene
03/01/23 01:400.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
03/01/23 01:402.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
03/01/23 01:400.5000.200<0.200µg/L1,2-Dibromoethane
03/01/23 01:400.5000.230<0.230µg/LDibromomethane
03/01/23 01:400.5000.220<0.220µg/L1,2-Dichlorobenzene
03/01/23 01:400.5000.190<0.190µg/L1,3-Dichlorobenzene
03/01/23 01:400.5000.210<0.210µg/L1,4-Dichlorobenzene
03/01/23 01:405.001.20<1.20µg/LDichlorodifluoromethane
03/01/23 01:400.5000.240<0.240µg/L1,1-Dichloroethane
Page 7 of 15Date:03/08/2023 02:20 PM
Page 128 of 140
Quality Control Data
23-055-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30378QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30377
Associated Lab Samples: 89757, 89758, 89759, 89760, 89761, 89762, 89763, 89764, 89765, 89766, 89767, 89768
LRB-V30377 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/01/23 01:400.5000.150<0.150µg/L1,2-Dichloroethane
03/01/23 01:400.5000.150<0.150µg/L1,1-Dichloroethene
03/01/23 01:400.5000.200<0.200µg/Lcis-1,2-Dichloroethene
03/01/23 01:400.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
03/01/23 01:400.5000.190<0.190µg/L1,2-Dichloropropane
03/01/23 01:400.5000.130<0.130µg/L1,3-Dichloropropane
03/01/23 01:402.000.210<0.210µg/L2,2-Dichloropropane
03/01/23 01:400.5000.200<0.200µg/L1,1-Dichloropropene
03/01/23 01:400.5000.210<0.210µg/Lcis-1,3-Dichloropropene
03/01/23 01:400.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
03/01/23 01:4020042.0<42.0µg/LEthanol
03/01/23 01:400.5000.170<0.170µg/LEthylbenzene
03/01/23 01:403.000.350<0.350µg/LHexachlorobutadiene
03/01/23 01:401.000.380<0.380µg/L2-Hexanone
03/01/23 01:400.5000.180<0.180µg/LIsopropylbenzene
03/01/23 01:400.5000.089<0.089µg/L4-Isopropyl toluene
03/01/23 01:405.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
03/01/23 01:401.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
03/01/23 01:401.000.078<0.078µg/L4-Methyl-2-Pentanone
03/01/23 01:402.000.330<0.330µg/LMethylene Chloride
03/01/23 01:401.000.470<0.470µg/LNaphthalene
03/01/23 01:400.5000.190<0.190µg/Ln-Propylbenzene
03/01/23 01:400.5000.220<0.220µg/LStyrene
03/01/23 01:4010.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
03/01/23 01:4010.00.350<0.350µg/Ltert-Butyl formate (TBF)
03/01/23 01:4010.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
03/01/23 01:4010.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 8 of 15Date:03/08/2023 02:20 PM
Page 129 of 140
Quality Control Data
23-055-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30378QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30377
Associated Lab Samples: 89757, 89758, 89759, 89760, 89761, 89762, 89763, 89764, 89765, 89766, 89767, 89768
LRB-V30377 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/01/23 01:400.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
03/01/23 01:400.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
03/01/23 01:400.5000.220<0.220µg/LTetrachloroethene
03/01/23 01:400.5000.220<0.220µg/LToluene
03/01/23 01:400.5000.380<0.380µg/L1,2,3-Trichlorobenzene
03/01/23 01:400.5000.310<0.310µg/L1,2,4-Trichlorobenzene
03/01/23 01:400.5000.160<0.160µg/L1,1,1-Trichloroethane
03/01/23 01:400.5000.096<0.096µg/L1,1,2-Trichloroethane
03/01/23 01:400.5000.180<0.180µg/LTrichloroethene
03/01/23 01:400.5000.180<0.180µg/LTrichlorofluoromethane
03/01/23 01:400.5000.270<0.270µg/L1,2,3-Trichloropropane
03/01/23 01:400.5000.190<0.190µg/L1,2,4-Trimethylbenzene
03/01/23 01:400.5000.180<0.180µg/L1,3,5-Trimethylbenzene
03/01/23 01:405.001.00<1.00µg/LVinyl Acetate
03/01/23 01:400.5000.170<0.170µg/LVinyl Chloride
03/01/23 01:400.5000.210<0.210µg/Lo-Xylene
03/01/23 01:401.000.420<0.420µg/Lm,p-Xylene
03/01/23 01:4010.01.00<1.00µg/L3,3-Dimethyl-1-butanol
03/01/23 01:404-Bromofluorobenzene (S)94.2 70-130
03/01/23 01:40Dibromofluoromethane (S)97.0 70-130
03/01/23 01:401,2-Dichloroethane - d4 (S)109 70-130
03/01/23 01:40Toluene-d8 (S)107 70-130
Page 9 of 15Date:03/08/2023 02:20 PM
Page 130 of 140
Quality Control Data
23-055-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30378QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30377
LCS-V30377 LCSD-V30377Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
39.2 98.095.538.240.0µg/LAcetone 40-160 2.5 20.0
17.6 88.088.017.620.0µg/LBenzene 70-130 0.0 20.0
18.3 91.593.018.620.0µg/LBromobenzene 70-130 1.6 20.0
17.6 88.089.017.820.0µg/LBromochloromethane 70-130 1.1 20.0
20.4 10210721.320.0µg/LBromodichloromethane 70-130 4.3 20.0
24.0 12012424.720.0µg/LBromomethane 60-140 2.8 20.0
16.7 83.585.017.020.0µg/Ln-Butylbenzene 70-130 1.7 20.0
15.6 78.084.016.820.0µg/Lsec-Butyl benzene 70-130 7.4 20.0
15.7 78.581.516.320.0µg/Ltert-Butyl benzene 70-130 3.7 20.0
20.0 10098.519.720.0µg/LCarbon Tetrachloride 70-130 1.5 20.0
18.6 93.097.519.520.0µg/LChlorobenzene 70-130 4.7 20.0
22.1 11111222.420.0µg/LChlorodibromomethane 70-130 1.3 20.0
23.8 11912224.420.0µg/LChloroethane 60-140 2.4 20.0
17.6 88.092.018.420.0µg/LChloroform 70-130 4.4 20.0
19.3 96.594.518.920.0µg/LChloromethane 60-140 2.0 20.0
16.9 84.590.018.020.0µg/L2-Chlorotoluene 70-130 6.3 20.0
17.6 88.092.518.520.0µg/L4-Chlorotoluene 70-130 4.9 20.0
19.2 96.096.519.320.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.5 20.0
19.0 95.096.519.320.0µg/L1,2-Dibromoethane 70-130 1.5 20.0
21.0 10510521.020.0µg/LDibromomethane 70-130 0.0 20.0
17.5 87.594.018.820.0µg/L1,2-Dichlorobenzene 70-130 7.1 20.0
17.5 87.589.017.820.0µg/L1,3-Dichlorobenzene 70-130 1.6 20.0
17.9 89.590.518.120.0µg/L1,4-Dichlorobenzene 70-130 1.1 20.0
14.6 73.072.014.420.0µg/LDichlorodifluoromethane 60-140 1.3 20.0
17.8 89.089.517.920.0µg/L1,1-Dichloroethane 70-130 0.5 20.0
22.4 11210621.120.0µg/L1,2-Dichloroethane 70-130 5.9 20.0
Page 10 of 15Date:03/08/2023 02:20 PM
Page 131 of 140
Quality Control Data
23-055-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30378QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30377
LCS-V30377 LCSD-V30377Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
17.6 88.091.518.320.0µg/L1,1-Dichloroethene 70-130 3.8 20.0
17.6 88.091.018.220.0µg/Lcis-1,2-Dichloroethene 70-130 3.3 20.0
17.6 88.089.517.920.0µg/Ltrans-1,2-Dichloroethene 70-130 1.6 20.0
19.1 95.595.019.020.0µg/L1,2-Dichloropropane 70-130 0.5 20.0
19.4 97.010020.020.0µg/L1,3-Dichloropropane 70-130 3.0 20.0
17.8 89.087.517.520.0µg/L2,2-Dichloropropane 70-130 1.6 20.0
17.2 86.085.017.020.0µg/L1,1-Dichloropropene 70-130 1.1 20.0
20.0 10098.519.720.0µg/Lcis-1,3-Dichloropropene 70-130 1.5 20.0
23.5 11811923.720.0µg/Ltrans-1,3-Dichloropropene 70-130 0.8 20.0
649 130122611500µg/LEthanol 60-140 6.0 20.0
19.1 95.597.519.520.0µg/LEthylbenzene 70-130 2.0 20.0
15.2 76.079.515.920.0µg/LHexachlorobutadiene 70-130 4.5 20.0
26.3 13213727.420.0µg/L2-Hexanone 60-140 4.0 20.0
15.6 78.080.516.120.0µg/LIsopropylbenzene 70-130 3.1 20.0
16.1 80.585.017.020.0µg/L4-Isopropyl toluene 70-130 5.4 20.0
24.9 12512124.220.0µg/LMethyl Ethyl Ketone (MEK)60-140 2.8 20.0
20.2 10199.019.820.0µg/LMethyl tert-butyl ether (MTBE)70-130 2.0 20.0
19.8 99.010020.020.0µg/LMethylene Chloride 70-130 1.0 20.0
18.5 92.593.018.620.0µg/LNaphthalene 70-130 0.5 20.0
15.5 77.583.016.620.0µg/Ln-Propylbenzene 70-130 6.8 20.0
18.3 91.593.018.620.0µg/LStyrene 70-130 1.6 20.0
45.8 11593.237.340.0µg/Ltert-Butyl Alcohol (TBA)40-140 20.4*20.0
54.5 13613955.740.0µg/Ltert-Butyl formate (TBF)40-140 2.1 20.0
24.1 12113025.920.0µg/Ltert-Amyl Alcohol (TAA)40-140 7.2 20.0
44.4 11111043.940.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 1.1 20.0
22.2 11111923.720.0µg/L1,1,1,2-Tetrachloroethane 70-130 6.5 20.0
Page 11 of 15* QC Fail Date:03/08/2023 02:20 PM
Page 132 of 140
Quality Control Data
23-055-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30378QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30377
LCS-V30377 LCSD-V30377Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.6 10811422.820.0µg/L1,1,2,2-Tetrachloroethane 70-130 5.4 20.0
16.9 84.584.516.920.0µg/LTetrachloroethene 70-130 0.0 20.0
22.1 11111021.920.0µg/LToluene 70-130 0.9 20.0
17.9 89.589.517.920.0µg/L1,2,3-Trichlorobenzene 70-130 0.0 20.0
17.2 86.090.018.020.0µg/L1,2,4-Trichlorobenzene 70-130 4.5 20.0
16.6 83.081.016.220.0µg/L1,1,1-Trichloroethane 70-130 2.4 20.0
22.0 11010721.420.0µg/L1,1,2-Trichloroethane 70-130 2.7 20.0
18.0 90.088.517.720.0µg/LTrichloroethene 70-130 1.6 20.0
21.2 10611322.520.0µg/LTrichlorofluoromethane 60-140 5.9 20.0
20.9 10511022.020.0µg/L1,2,3-Trichloropropane 70-130 5.1 20.0
16.4 82.086.517.320.0µg/L1,2,4-Trimethylbenzene 70-130 5.3 20.0
17.2 86.088.517.720.0µg/L1,3,5-Trimethylbenzene 70-130 2.8 20.0
27.2 136142*28.420.0µg/LVinyl Acetate 60-140 4.3 20.0
19.7 98.598.019.620.0µg/LVinyl Chloride 60-140 0.5 20.0
17.5 87.587.017.420.0µg/Lo-Xylene 70-130 0.5 20.0
39.2 98.099.739.940.0µg/Lm,p-Xylene 70-130 1.7 20.0
17.9 89.598.019.620.0µg/L3,3-Dimethyl-1-butanol 70-130 9.0 20.0
87.489.64-Bromofluorobenzene (S)70-130
93.493.6Dibromofluoromethane (S)70-130
1161151,2-Dichloroethane - d4 (S)70-130
99.8100Toluene-d8 (S)70-130
Page 12 of 15* QC Fail Date:03/08/2023 02:20 PM
Page 133 of 140
Quality Control Data
23-055-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30431QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30429
Associated Lab Samples: 89749, 89753, 89754, 89766, 89767
LRB-V30429 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/01/23 23:320.5000.180<0.180µg/LBenzene
03/01/23 23:320.5000.170<0.170µg/LEthylbenzene
03/01/23 23:321.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
03/01/23 23:321.000.470<0.470µg/LNaphthalene
03/01/23 23:3210.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
03/01/23 23:3210.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
03/01/23 23:320.5000.220<0.220µg/LToluene
03/01/23 23:320.5000.190<0.190µg/L1,2,4-Trimethylbenzene
03/01/23 23:320.5000.180<0.180µg/L1,3,5-Trimethylbenzene
03/01/23 23:320.5000.210<0.210µg/Lo-Xylene
03/01/23 23:321.000.420<0.420µg/Lm,p-Xylene
03/01/23 23:324-Bromofluorobenzene (S)101 70-130
03/01/23 23:32Dibromofluoromethane (S)101 70-130
03/01/23 23:321,2-Dichloroethane - d4 (S)96.4 70-130
03/01/23 23:32Toluene-d8 (S)100 70-130
LCS-V30429 LCSD-V30429Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.4 10210320.520.0µg/LBenzene 70-130 0.4 20.0
19.8 99.099.019.820.0µg/LEthylbenzene 70-130 0.0 20.0
20.0 10096.019.220.0µg/LMethyl tert-butyl ether (MTBE)70-130 4.0 20.0
22.8 11499.519.920.0µg/LNaphthalene 70-130 13.5 20.0
43.3 10894.737.940.0µg/Ltert-Butyl Alcohol (TBA)40-140 13.3 20.0
23.3 11711623.220.0µg/Ltert-Amyl Alcohol (TAA)40-140 0.4 20.0
20.1 10110120.220.0µg/LToluene 70-130 0.4 20.0
Page 13 of 15Date:03/08/2023 02:20 PM
Page 134 of 140
Quality Control Data
23-055-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30431QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30429
LCS-V30429 LCSD-V30429Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.8 99.099.019.820.0µg/L1,2,4-Trimethylbenzene 70-130 0.0 20.0
19.6 98.099.519.920.0µg/L1,3,5-Trimethylbenzene 70-130 1.5 20.0
19.9 99.598.019.620.0µg/Lo-Xylene 70-130 1.5 20.0
39.9 99.710240.740.0µg/Lm,p-Xylene 70-130 1.9 20.0
96.41024-Bromofluorobenzene (S)70-130
10099.4Dibromofluoromethane (S)70-130
1041021,2-Dichloroethane - d4 (S)70-130
10099.6Toluene-d8 (S)70-130
Page 14 of 15Date:03/08/2023 02:20 PM
Page 135 of 140
Quality Control Data
23-055-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #10
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30528QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30526
Associated Lab Samples: 89759
LRB-V30526 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/07/23 03:200.5000.220<0.220µg/LToluene
03/07/23 03:204-Bromofluorobenzene (S)95.2 70-130
03/07/23 03:20Dibromofluoromethane (S)96.0 70-130
03/07/23 03:201,2-Dichloroethane - d4 (S)86.4 70-130
03/07/23 03:20Toluene-d8 (S)95.4 70-130
LCS-V30526 LCSD-V30526Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.0 95.098.019.620.0µg/LToluene 70-130 3.1 20.0
93.096.04-Bromofluorobenzene (S)70-130
98.698.2Dibromofluoromethane (S)70-130
88.486.61,2-Dichloroethane - d4 (S)70-130
95.095.0Toluene-d8 (S)70-130
Page 15 of 15Date:03/08/2023 02:20 PM
Page 136 of 140
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-055-0021
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 1.5C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Danyale Love Date & Time:02/24/2023 15:41:40
Special precautions or instructions included?
Comments:
Page 137 of 140
Page 138 of 140
Page 139 of 140
Page 140 of 140

APPENDIX F
Contaminant Mass Calculations
Area ID Well IDs
Area
(ft²)
Average Well
Depth
(ft)
Average
Depth to
Water
(ft)
Water Column
Height
(ft)
Volume
(ft³)
Volume
(L)
Effective
Porosity
Effective
Volume
(L)
1 MW-15 2,141.38 35 22.23 12.77 27,345 774,335 232,300
2 MW-1 1,787.82 40 29.61 10.39 18,575 525,997 157,799
MW-2
MW-9
MW-5
MW-14
MW-8
MW-11
6 MW-3 15,324.54 40 29.83 10.17 155,851 4,413,189 1,323,957
Area Date Well
Benzene
(µ/L)
Toluene
(µ/L)
Ethylbenzene
(µ/L)
Xylenes
(µ/L)
MTBE
(µ/L)
Naphthalene
(µ/L)
Total
(µ/L)
DTW
(ft)
Average Water
Column Height
(ft)
Total Average Mass
(g)Percent Change To Date Change
11/30/17 13,400.00 13,400.00 1,230.00 5,370.00 433.00 264.00 34,097.00 22.23 12.77 7,920.75 ------
10/25/18 8,650.00 9,600.00 1,030.00 4,960.00 689.00 282.00 25,211.00 20.76 14.24 6,530.69 17.5%17.5%
01/07/19 6,500.00 8,270.00 926.00 4,480.00 724.00 208.00 21,108.00 18.91 16.09 6,178.20 5.4%22.0%
03/25/19 NS NS NS NS NS NS NS NS NS n/a n/a n/a
05/08/19 7,400.00 8,170.00 970.00 4,530.00 906.00 268.00 22,244.00 17.54 17.46 7,065.07 -14.4%10.8%
05/20/20 0.00 0.00 0.00 0.00 0.00 0.00 0.00 17.93 17.07 0.00 100.0%100.0%
12/01/20 9,450 10,500.00 1,190.00 5,910.00 1,390.00 251.00 28,691.00 17.17 17.83 9,305.85 ----17.5%
06/14/21 9,660.00 12,000.00 1,100.00 5,640.00 1,280.00 231.00 29,911.00 16.91 18.09 9,843.03 -5.8%-24.3%
06/21/22 7,100 8,160 899 4,390 1,150 534 22,233 19.62 15.38 6,220.33 36.8%21.5%
02/13/23 7,610 8,480 985 4,720 1,280 422 23,497 18.82 16.18 6,915.92 -11.2%12.7%
05/26/17 22,800.00 37,400.00 3,810.00 18,400.00 1,120.00 1,030.00 84,560.00 29.61 10.39 13,343.50 ------
05/22/18 FP FP FP FP FP FP FP 29.68 10.32 n/a n/a n/a
01/07/19 11,900.00 21,700.00 2,700.00 11,500.00 289.00 1,150.00 49,239.00 26.57 13.43 10,043.25 24.7%24.7%
03/25/19 14,800.00 31,800.00 3,030.00 15,000.00 1,400.00 556.00 66,586.00 24.90 15.10 15,270.35 -52.0%-14.4%
05/08/19 19,700.00 33,500.00 3,600.00 17,900.00 1,040.00 954.00 76,694.00 24.71 15.29 17,806.27 -16.6%-33.4%
05/20/20 FP FP FP FP FP FP FP 25.11 14.89 n/a n/a n/a
12/01/20 9980.00 27,200.00 2,840.00 15,300.00 0.00 968.00 56,288.00 25.36 14.64 12,515.44 29.7%6.2%
06/14/21 8,260.00 53,700.00 25,400.00 172,000.00 0.00 65,800.00 325,160.00 24.21 15.79 77,977.35 -523.0%-484.4%
06/21/22 13,200 39,200 2,810 13,600 427 1,050 70,287 26.87 13.13 14,016.16 82.0%-5.0%
02/13/23 FP FP FP FP FP FP FP 27.11 12.89 n/a n/a n/a
13,742.17 35 23.25 4,572,328
5,059,688
1,371,698
1,517,906178,681
161,470
APPENDIX F
CONTAMINANT MASS CALCULATIONS
KINGSWAY #10 (INCIDENT NO. 40626)
3 8,943.20 40 30.12 9.88
5 16,637.01 40 29.26 10.74
Baseline Event
88,359
0.30
2,502,039 750,612
11.754
Area 1 MW-15
Area 2 MW-1
Page 1 of 5
Area ID Well IDs
Area
(ft²)
Average Well
Depth
(ft)
Average
Depth to
Water
(ft)
Water Column
Height
(ft)
Volume
(ft³)
Volume
(L)
Effective
Porosity
Effective
Volume
(L)
1 MW-15 2,141.38 35 22.23 12.77 27,345 774,335 232,300
2 MW-1 1,787.82 40 29.61 10.39 18,575 525,997 157,799
MW-2
MW-9
MW-5
MW-14
MW-8
MW-11
6 MW-3 15,324.54 40 29.83 10.17 155,851 4,413,189 1,323,957
Area Date Well
Benzene
(µ/L)
Toluene
(µ/L)
Ethylbenzene
(µ/L)
Xylenes
(µ/L)
MTBE
(µ/L)
Naphthalene
(µ/L)
Total
(µ/L)
DTW
(ft)
Average Water
Column Height
(ft)
Total Average Mass
(g)Percent Change To Date Change
13,742.17 35 23.25 4,572,328
5,059,688
1,371,698
1,517,906178,681
161,470
APPENDIX F
CONTAMINANT MASS CALCULATIONS
KINGSWAY #10 (INCIDENT NO. 40626)
3 8,943.20 40 30.12 9.88
5 16,637.01 40 29.26 10.74
Baseline Event
88,359
0.30
2,502,039 750,612
11.754
MW-2 FP FP FP FP FP FP FP 30.37
MW-9 8,890.00 20,800.00 3,570.00 17,800.00 2,450.00 1,470.00 54,980.00 30.08
Avg.8,890.00 20,800.00 3,570.00 17,800.00 2,450.00 1,470.00 54,980.00 30.23
MW-2 9,590.00 15,700.00 2,130.00 11,120.00 1,870.00 769.00 41,179.00 28.98
MW-9 7,170.00 12,500.00 1,430.00 7,190.00 1,690.00 472.00 30,452.00 28.88
Avg.8,380.00 14,100.00 1,780.00 9,155.00 1,780.00 620.50 35,815.50 28.93
MW-2 2,120.00 3,610.00 938.00 4,800.00 441.00 388.00 12,297.00 27.13
MW-9 14,000.00 19,500.00 1,950.00 9,350.00 1,610.00 635.00 47,045.00 26.97
Avg.8,060.00 11,555.00 1,444.00 7,075.00 1,025.50 511.50 29,671.00 27.05
MW-2 2,740.00 3,960.00 1,010.00 5,350.00 536.00 464.00 14,060.00 25.48
MW-9 967.00 953.00 144.00 839.00 124.00 68.10 3,095.10 25.31
Avg.1,853.50 2,456.50 577.00 3,094.50 330.00 266.05 8,577.55 25.40
MW-2 9,840.00 12,000.00 1,390.00 6,910.00 1,760.00 493.00 32,393.00 25.26
MW-9 3,930.00 4,420.00 451.00 2,560.00 165.00 258.00 11,784.00 25.16
Avg.6,885.00 8,210.00 920.50 4,735.00 962.50 375.50 22,088.50 25.21
MW-2 FP FP FP FP FP FP FP 26.02
MW-9 1,330.00 1,840.00 179.00 1,050.00 67.10 88.10 4,554.20 26.21
Avg.n/a n/a n/a n/a n/a n/a n/a 26.12
MW-2 3140.00 5,650.00 1,140.00 6,000.00 362.00 555.00 16,847.00 25.75
MW-9 10200.00 18,300.00 1,490.00 7,440.00 912.00 361.00 38,703.00 25.68
Avg.6,670.00 11,975.00 1,315.00 6,720.00 637.00 458.00 27,775.00 25.72
MW-2 3,470.00 6,280.00 1,050.00 5,680.00 353.00 416.00 17,249.00 24.69
MW-9 12,300.00 16,500.00 1,360.00 6,860.00 631.00 288.00 37,939.00 24.62
Avg.7,885.00 11,390.00 1,205.00 6,270.00 492.00 352.00 27,594.00 24.66
MW-2 FP FP FP FP FP FP FP 27.15
MW-9 6,280 13,500 1,450 7,150 0 532 28,912 26.93
Avg.6,280 13,500 1,450 7,150 0 532 28,912 27.04
MW-2 FP FP FP FP FP FP FP 27.21
MW-9 5,230 9,000 1,230 5,530 158 427 21,575 27.01
Avg. 5,230 9,000 1,230 5,530 158 427 21,575 27.11
14.29 30,143.43 -527.4%26.2%
11.5% 30.3%
14.61
80.6%
29,191.76 3.1%
26.2%30,121.53
9.78 40,830.05 ---
32,169.18
67.4%
---09/26/17
01/07/19
-160.8%05/08/19 14.79 24,819.49
05/20/20 4,804.15
-6.7% -157.0%
88.2%13.89
12/01/20
02/13/23 12.89 21,128.18 25.8% 48.3%
Area 3
06/21/22 12.96 28,466.99
11.0710/25/18
12.95
06/14/21 15.35
26.2%
28.5%
39.2%
76.7%03/25/19 9,517.51
Page 2 of 5
Area ID Well IDs
Area
(ft²)
Average Well
Depth
(ft)
Average
Depth to
Water
(ft)
Water Column
Height
(ft)
Volume
(ft³)
Volume
(L)
Effective
Porosity
Effective
Volume
(L)
1 MW-15 2,141.38 35 22.23 12.77 27,345 774,335 232,300
2 MW-1 1,787.82 40 29.61 10.39 18,575 525,997 157,799
MW-2
MW-9
MW-5
MW-14
MW-8
MW-11
6 MW-3 15,324.54 40 29.83 10.17 155,851 4,413,189 1,323,957
Area Date Well
Benzene
(µ/L)
Toluene
(µ/L)
Ethylbenzene
(µ/L)
Xylenes
(µ/L)
MTBE
(µ/L)
Naphthalene
(µ/L)
Total
(µ/L)
DTW
(ft)
Average Water
Column Height
(ft)
Total Average Mass
(g)Percent Change To Date Change
13,742.17 35 23.25 4,572,328
5,059,688
1,371,698
1,517,906178,681
161,470
APPENDIX F
CONTAMINANT MASS CALCULATIONS
KINGSWAY #10 (INCIDENT NO. 40626)
3 8,943.20 40 30.12 9.88
5 16,637.01 40 29.26 10.74
Baseline Event
88,359
0.30
2,502,039 750,612
11.754
MW-5 341.00 120.00 61.30 496.00 506.00 15.10 1,539.40 29.21
MW-14 169.00 11.20 31.80 148.00 19.30 2.10 381.40 17.29
Avg.255.00 9,602.18 46.55 322.00 262.65 8.60 960.40 23.25
MW-5 NS NS NS NS NS NS NS NS
MW-14 48.30 2.10 11.50 54.60 16.60 1.60 134.70 15.76
Avg.n/a n/a n/a n/a n/a n/a n/a n/a
MW-5 NS NS NS NS NS NS NS NS
MW-14 NS NS NS NS NS NS NS NS
Avg.n/a n/a n/a n/a n/a n/a n/a n/a
MW-5 NS NS NS NS NS NS NS NS
MW-14 24.10 1.60 6.90 32.10 9.80 0.74 75.24 13.78
Avg.n/a n/a n/a n/a n/a n/a n/a n/a
MW-5 NS NS NS NS NS NS NS NS
MW-14 95.20 5.40 25.80 120.00 26.40 3.20 276.00 12.55
Avg.n/a n/a n/a n/a n/a n/a n/a n/a
MW-5 NS NS NS NS NS NS NS NS
MW-14 0.00 0.00 0.00 0.00 0.00 0.00 0.00 13.27
Avg.n/a n/a n/a n/a n/a n/a n/a n/a
MW-5 NS NS NS NS NS NS NS NS
MW-14 0.15 0.18 0.00 0.00 1.80 0.00 2.13 12.71
Avg.0.15 0.18 0.00 0.00 1.80 0.00 2.13 12.71
MW-5 183.00 141.00 80.50 397.00 1,050.00 6.40 1,857.90 23.91
MW-14 0.00 0.00 0.00 0.00 2.60 0.00 2.60 11.83
Avg.91.50 70.50 40.25 198.50 526.30 3.20 930.25 17.87
MW-5 1760.00 656.00 802.00 3,750.00 10,600.00 119.00 17,687.00 26.62
MW-14 0 0 0 0 1.70 0.13 1.83 13.75
Avg.880 328 401 1875 5,300.85 59.57 8844.42 20.19
MW-5 92.40 18.70 32.80 178.00 669.00 9.72 1,000.62 26.75
MW-14 0 0 0 0 1.62 0.00 1.62 13.65
Avg. 46.2 9.35 16.4 89.0 335.31 4.86 501.12 20.20
12/01/20 22.29 5.54 99.2% 99.6%
-722.3% -1061.1%
21.22
02/13/23 14.80 865.81 94.3%
0.00 100.0%
01/07/19 n/a
100.0%
n/a n/an/a
---
06/14/21 17.13 1,860.28 -33463.5% -41.2%
11.75
19.24
1,317.38
-288.1%
---
05/08/19
10/25/18
21.7305/20/20
5/26/2017 &
11/30/17
03/25/19 85.9%
77.0%
186.39 38.4%
22.45 723.35 45.1%
302.55 77.0%
34.3%
Area 4
06/21/22 14.82 15,296.48
Page 3 of 5
Area ID Well IDs
Area
(ft²)
Average Well
Depth
(ft)
Average
Depth to
Water
(ft)
Water Column
Height
(ft)
Volume
(ft³)
Volume
(L)
Effective
Porosity
Effective
Volume
(L)
1 MW-15 2,141.38 35 22.23 12.77 27,345 774,335 232,300
2 MW-1 1,787.82 40 29.61 10.39 18,575 525,997 157,799
MW-2
MW-9
MW-5
MW-14
MW-8
MW-11
6 MW-3 15,324.54 40 29.83 10.17 155,851 4,413,189 1,323,957
Area Date Well
Benzene
(µ/L)
Toluene
(µ/L)
Ethylbenzene
(µ/L)
Xylenes
(µ/L)
MTBE
(µ/L)
Naphthalene
(µ/L)
Total
(µ/L)
DTW
(ft)
Average Water
Column Height
(ft)
Total Average Mass
(g)Percent Change To Date Change
13,742.17 35 23.25 4,572,328
5,059,688
1,371,698
1,517,906178,681
161,470
APPENDIX F
CONTAMINANT MASS CALCULATIONS
KINGSWAY #10 (INCIDENT NO. 40626)
3 8,943.20 40 30.12 9.88
5 16,637.01 40 29.26 10.74
Baseline Event
88,359
0.30
2,502,039 750,612
11.754
MW-8 66.10 4.40 21.60 398.00 249.00 42.20 781.30 29.27
MW-11 47.80 0.26 0.79 16.30 0.00 1.10 66.25 28.68
Avg.56.95 2.33 11.20 207.15 124.50 21.65 423.78 28.98
MW-8 NS NS NS NS NS NS NS NS
MW-11 NS NS NS NS NS NS NS NS
Avg.n/a n/a n/a n/a n/a n/a n/a n/a
MW-8 NS NS NS NS NS NS NS NS
MW-11 NS NS NS NS NS NS NS NS
Avg.n/a n/a n/a n/a n/a n/a n/a n/a
MW-8 NS NS NS NS NS NS NS NS
MW-11 NS NS NS NS NS NS NS NS
Avg.n/a n/a n/a n/a n/a n/a n/a n/a
MW-8 NS NS NS NS NS NS NS NS
MW-11 NS NS NS NS NS NS NS NS
Avg.n/a n/a n/a n/a n/a n/a n/a n/a
MW-8 NS NS NS NS NS NS NS NS
MW-11 NS NS NS NS NS NS NS NS
Avg.n/a n/a n/a n/a n/a n/a n/a n/a
MW-8 NS NS NS NS NS NS NS NS
MW-11 NS NS NS NS NS NS NS NS
Avg.n/a n/a n/a n/a n/a n/a n/a n/a
MW-8 3.60 0.25 1.10 28.60 10.90 0.68 45.13 24.49
MW-11 14.30 0.00 0.22 7.90 0.00 1.00 23.42 22.75
Avg.8.95 0.13 0.66 18.25 5.45 0.84 34.28 23.62
MW-8 2.5 0.0 0.7 21.0 12.7 0.6 37.51 26.20
MW-11 10.2 0.0 0.2 6.1 0.0 1.2 17.69 25.37
Avg.6.4 0.0 0.5 13.6 6.4 0.9 27.60 25.79
MW-8 0.941 0.0 0.697 11.7 19.2 0.0 32.54 26.30
MW-11 19.0 0.0 0.648 8.80 0.0 1.32 29.77 25.08
Avg. 9.97 0.0 0.673 10.25 9.6 0.66 31.15 25.69
n/a
30.1% 91.6%
88.0%79.3516.38
10/25/18
01/07/19
12/01/20 n/a n/a n/a
n/a n/a05/20/20 n/a
n/a
n/a
660.32 ---
n/a
n/a
n/a n/a n/a
n/a
n/a n/a n/a
n/a
06/14/21 88.0%
03/25/19
n/a n/a n/a
11.039/26/2017 &
11/30/17 ---
05/08/19 n/a
n/a
02/13/23 14.31 63.01 -13.6%90.5%
Area 5
06/21/22 14.22 55.45
Page 4 of 5
Area ID Well IDs
Area
(ft²)
Average Well
Depth
(ft)
Average
Depth to
Water
(ft)
Water Column
Height
(ft)
Volume
(ft³)
Volume
(L)
Effective
Porosity
Effective
Volume
(L)
1 MW-15 2,141.38 35 22.23 12.77 27,345 774,335 232,300
2 MW-1 1,787.82 40 29.61 10.39 18,575 525,997 157,799
MW-2
MW-9
MW-5
MW-14
MW-8
MW-11
6 MW-3 15,324.54 40 29.83 10.17 155,851 4,413,189 1,323,957
Area Date Well
Benzene
(µ/L)
Toluene
(µ/L)
Ethylbenzene
(µ/L)
Xylenes
(µ/L)
MTBE
(µ/L)
Naphthalene
(µ/L)
Total
(µ/L)
DTW
(ft)
Average Water
Column Height
(ft)
Total Average Mass
(g)Percent Change To Date Change
13,742.17 35 23.25 4,572,328
5,059,688
1,371,698
1,517,906178,681
161,470
APPENDIX F
CONTAMINANT MASS CALCULATIONS
KINGSWAY #10 (INCIDENT NO. 40626)
3 8,943.20 40 30.12 9.88
5 16,637.01 40 29.26 10.74
Baseline Event
88,359
0.30
2,502,039 750,612
11.754
05/26/17 MW-3 8.00 45.10 18.90 96.50 0.68 12.30 181.48 29.83 10.17 240.27 --- ---
10/25/18 MW-3 NS NS NS NS NS NS NS NS n/a n/a n/a n/a
01/07/19 MW-3 NS NS NS NS NS NS NS NS n/a n/a n/a n/a
03/25/19 MW-3 NS NS NS NS NS NS NS NS n/a n/a n/a n/a
05/08/19 MW-3 NS NS NS NS NS NS NS NS n/a n/a n/a n/a
05/20/20 MW-3 NS NS NS NS NS NS NS NS n/a n/a n/a n/a
12/01/20 MW-3 NS NS NS NS NS NS NS NS n/a n/a n/a n/a
06/14/21 MW-3 0.00 0.00 0.00 0.00 0.57 0.00 0.57 24.84 15.16 1.12 99.5%99.5%
06/21/22 MW-3 NS NS NS NS NS NS NS NS n/a n/a n/a n/a
02/13/23 MW-3 0.00 0.00 0.00 0.00 0.00 0.00 0.00 27.21 12.79 0.00 100.0% 100.0%
Date
Average Water
Column Height
(ft)
05/26/17,
09/26/17 or
11/30/17
10.98 64,312.27
10/25/18 14.85 37,855.36
01/07/19 14.16 46,616.36
03/25/19 16.98 32,053.04
05/08/19 17.50 51,314.76
05/20/20 16.89 23,511.01
12/01/20 17.26 52,870.86
06/14/21 16.32 121,930.30
06/21/22 14.10 64,056.53
02/13/23 13.98 42,989.08
Notes:
• Area of the contaminant plume is calculated from Figure #6.
• FP: Free Product
• NS: Not Sampled
• n/a: Not Avaliable due to not being sample or presence of free product
• Height of the water column is calculated by subtracting the average depth to water from the average well depth of the referenced monitoring wells
• Volume of the contaminant plume is calculated by multiplying the area of the plume by the average height of the water column during each sampling event
• Effective porosity is assumed based on the sub-surface soil profile obtained from well construction records and soil boring logs
• Total mass was calculated by multiplying the total contaminant concentrations for the sampling event with effective volume
• Contaminant mass cannot be calculated in wells containing FP; therefore, the total contaminant mass is based on the known concentrations in the area for each sampling event.
• When areas couldn’t be sampled, the last known concentrations were used in the calculations.
-124.88%17.79%
Total Contaminant Mass
(g)
63.44%
-60.09%20.21%
Percent Change Compared to
Previous Event
---
41.14%
-23.14%
31.24%
54.18%
Percent Change To Date
50.16%
32.89%33.16%
Area 6
47.46%0.40%
-130.62%-89.59%
---
41.14%
27.52%
Page 5 of 5

APPENDIX G
MMPE Report and Disposal Manifests

ADVANCED
ENVIRONMENTAL SERVICES, INC.
“Your Environmental Solutions Partner”

MOBILE
MULTI-PHASE
EXTRACTION REPORT

Site Location:

Kingsway #10
1418 W. Garrison Blvd.
Gastonia, NC

Prepared for:

Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
PM – Ms. Joanna Alley

February 1, 2023

TABLE OF CONTENTS

EVENT SUMMARY

MMPE FIELD LOG

MASS-REMOVAL CALCULATION

FIELD NOTES

DISPOSAL MANIFESTS

MOBILE MULTI-PHASE EXTRACTION
EVENT SUMMARY

February 1, 2023

Location: Kingsway #10
1418 W. Garrison Blvd.
Gastonia, NC

Client: Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110

Event Dates: January 9 – 13, 2023
Advanced Job # 01 - 2301

Advanced Personnel: Lee Heilig, Chad Widner, Gary McDaniel, and Scott Crook

MMPE System: MMPE systems rated 21” hg at 130 CFM – 2” Diameter Stack
and 25” hg at 280 CFM - 6” diameter
5,000 - gallon tanker and 6,000 gallon tanker
200’ piping 1.5” hose to 4 wells

Extraction Well: MW-2, RW-1, RW-2 and RW-3

Well Initial FP / WL(ft) Final FP / WL(ft) Stinger depth(ft) Run Time
/ Changed To
MW-2 28.00/28.03 31.54 28 96.0 hours
RW-1 27.90 30.24 28 96.0 hours
RW-2 28.17 30.28 28 96.0 hours
RW-3 27.72 30.80 28 96.0 hours

Description of Event:
The MMPE event ran from 12:00 January 9, 2023, through 12:00 January 13, 2023. The MMPE systems
was active for 96.0 hours. During the event vacuum at the recovery pump maintained 23.0 inches of
mercury (hg) on System A, and ranged from 14.0 to 15.0 inches of mercury (hg) on system B, and
stabilized at approximately 23.0 and 15.0 inches of mercury respectively. Airflow rates maintained 1,100
feet per minute on System A and ranged from 3,600 to 3,800 feet per minute on System B, and stabilized at
approximately 1,100 feet per minute on System A, and 3,600 feet per minute on System B. System
temperature ranged from 108 – 124 degrees F on System A and 102 – 120 degrees F on System B.
Humidity ranged from 56 to 72 percent on System A, and maintained 99 percent on System B. Field
gauged volatile organic compounds (VOC’s) decreased from 5,500 parts per-million (PPM) to 1,900
parts per-million (PPM) on System A, and decreased from 1,400 parts per-million (PPM) to 600
parts per-million on System B.

Groundwater / Product Mix Recovered:
During the event a total of 9,495 gallons of product/water mix were removed from the site and properly
disposed at a certified North Carolina disposal facility. Total fluids recovered, was measured based on stick
readings conducted during and following the event. Based on 96.0 hours of operation and a total of
9,495gallons recovered during the event, the average groundwater recovery rate was calculated to be
approximately 98.91 gallons per hour.

Events Results:
Based on mass-removal calculations 112.39 pounds or 18.27 gallons of VOC’s were removed as vapor on
System A, and 13.35 pounds or 2.7 gallons of VOC’s were removed as vapor on System B. During the
event, vacuum influence and drawdown were measured at MW-1, MW-3 and MW-9. Vacuum influence
at MW-1 and MW-9 measured 2.70 and 5.0+ inches of water, respectively. Drawdown at MW-1,
MW-3 and MW-9 measured 1.07, 0.38 and 2.39 feet, respectively. Following the event, no free
product was identified in any well.

MMPE FIELD LOG:
CLIENT: Geological Resources Inc.
JOB NAME: Kingsway #10 System A
LOCATION: Gastonia, NC
MMPE EVENT DATES: January 9 - 13, 2023
EXTRACTION POINTS: RW-1 and MW-2
AES JOB NUMBER: 01 - 2301
DATE TIME FLOW (f/m) HUM.(%) TEMP. (F)VOC's(ppm)VAC. (hg")GALLONS STINGER/WL's EXTRACTION POINTS (hg")
RW-1 MW-2
Stinger(ft)28 28
Start 12:00 Initial WL's 27.90 28.00/28.03

01/09/23 12:30 1,100 72.0 108 5,500 23.0 18.0 18.0
13:30 1,100 62.0 118 5,200 23.0 18.0 18.0
18:20 1,100 60.0 120 3,600 23.0 18.0 18.0
19:20 1,100 60.0 120 3,500 23.0 18.0 18.0
01/10/23 8:30 1,100 60.0 120 2,500 23.0 1.260 gal.18.0 18.0
10:30 1,100 58.0 122 2,500 23.0 18.0 18.0
16:10 1,100 56.0 124 2,400 23.0 18.0 18.0
18:10 1,100 58.0 122 2,400 23.0 18.0 18.0
01/11/23 8:40 1,100 60.0 120 2,200 23.0 18.0 18.0
10:40 1,100 58.0 122 2,200 23.0 18.0 18.0
12:40 1,100 56.0 124 2,100 23.0 3,000 gal.18.0 18.0
17:10 1,100 56.0 124 2,100 23.0 18.0 18.0
01/12/23 8:10 1,100 60.0 120 2,000 23.0 18.0 18.0
10:30 1,100 60.0 120 2,000 23.0 18.0 18.0
12:30 1,100 60.0 120 2,000 23.0 P/O 4,350 18.0 18.0
16:30 1,100 56.0 124 2,000 23.0 18.0 18.0
01/13/23 10:10 1,100 60.0 120 1,900 23.0 18.0 18.0
11:10 1,100 60.0 120 1,900 23.0 18.0 18.0
End 12:00 Final WL's 30.24 31.54
Total fluids: 5,810 gal.
Total free product:0 gal.
DATE TIME STINGER/WL's EXTRACTION POINTS (hg") cont. VACUUM INFLUENCE (h2o") WELL GAUGING (ft)
MW-1 MW-1
Stinger(ft)
Initial WL's
01/09/23 12:30 0.00 27.98
13:30
18:20
19:20
01/10/23 8:30
10:30 2.60 28.60
16:10
18:10
01/11/23 8:40
10:40
12:40 2.70 28.98
17:10
01/12/23 8:10
10:30
12:30 2.70 29.02
16:30
01/13/23 10:10
11:10 2.70 29.05
End 12:00
Page 1 of 1
MOBILE MULTI-PHASE EXTRACTION EVENT
SITE NAME: Kingsway #10 System A CLIENT: Geological Resources
INCIDENT NUMBER:
AVERAGE DEPTH TO GROUNDWATER: 27 - 29 feet
DESCRIBE SOIL IN THE SATURATED ZONE:
AVERAGE HYDRAULIC CONDUCTIVITY (if known):
EXTRACTION WELLS USED FOR MMPE: RW-1 and MW-2
SPECIFICATIONS OF THE MMPE SYSTEM (cfm @ in Hg): 280 cfm @ 25.0"Hg
DRY STANDARD CUBIC FEET PER MINUTE (DSCFM) AIR FLOW CALCULATIONS (Qstd)
Date Hours Vacuum Velocity Pipe ID Temp Rel Humid Water Water Qstd(inches of Hg)(ft/min)(in)(°F)(%)Vapor (Wt%)Vapor (Vol%)(flow)
1/9/23 24.00 23.00 1100.00 6 117 63.5 0.044 0.066 185
1/10/23 48.00 23.00 1100.00 6 122 58.0 0.049 0.073 182
1/11/23 72.00 23.00 1100.00 6 122 57.5 0.048 0.071 182
1/12/23 96.00 23.00 1100.00 6 121 59.5 0.051 0.076 182
1/13/23
NOTES
Qstd = Flow at DSCFM
Vacuum = The level of vacuum being applied should be recorded from the MMPE system (inches of Hg)
Velocity = The rate at which air flows is measured at the blower discharge piping (anemometer or pitot tube)
Pipe ID = The inside diameter of the blower discharge piping (from the MMPE system)
Temperature = The temperature of the air stream exiting the blower discharge piping (dry bulb temp., in deg.°F)Relative humidity = The % relative humidity of the air stream exiting the blower discharge piping
Bwsw = water vapor % by weight, i.e., pounds of water per pound of dry air, derived from the Psychrometric chart (temp Vs relative humidity)
Bws = water vapor % by volume
EQUATIONS
Bws = (Bwsw/18 lb-mole H20)/[(1/28.84 lb-mole dry air) + (Bwsw/18 lb-mole H2O)]Qstd = (1-Water Vapor) * velocity * (PI * (diameter/24)2) * (528°R/(Temp + 460))
EMISSION CALCULATIONS
Elapsed
Time Flow PPMmeasured PPMwet PPMdry K PPMconc Cc:m Cc PMRc PMRg PMR
(hour)(DSCFM)(ppm)(#C - gas)(mg/dsm3)(lb/dscf)(lb/hour)(lb/hour)(lb)
24 185 4450 4450 4764 1 4764 2377 0.00014839 1.65 1.90 45.70
48 182 2450 2450 2642 1 2642 1318 8.23095E-05 0.90 1.04 24.92
72 182 2150 2150 2315 1 2315 1155 7.21235E-05 0.79 0.91 21.89
96 182 1950 1950 2109 1 2109 1052 6.57063E-05 0.72 0.83 19.89
Total emissions in pounds 112.39
Total emissions as gallons (pounds / 6.152)18.27
NOTES
PPMmeasured = Actual measurements (ppm) taken with a OVA or TVA at the blower discharge piping
PPMwet = "wet" concentration
PPMdry = "dry" concentration
K = Number of carbons in calibration gas: (Methane K = 1, or Propane K = 3, or Hexane K = 6)
PPMc= PPMv, Volumetric concentration of VOC emissions as carbon, dry basis at STP
Cc:m = mg/dsm3, mass concentration of VOC emissions as carbon
Mc = 12.01 mg/mg-mole, molecular weight of carbon
K3 = 24.07 dsm3/106 mg-mole, mass to volume conversion factor at STP
Cc = lb/dcsf, mass concentration of VOC emissions as carbon, dry basis at STP
PMRc = lb/hr, pollutant mass removal rate of VOC's as carbon
PMRg = lb/hr, pollutant mass removal rate of of VOC's as gasolinePMR = lb, pollutant mass removal of VOC's as gasoline
EQUATIONS
PPMwet = PPMmeasuredPPMdry = (PPMwet)/(1-Bws)
PPMc = (PPMd)(K)
Cc:m = (PPMc)(Mc / K3)Cc = (Cc:m)(62.43x10-9 lb-m3/mg-ft3)
PMRc = (Cc)(Qstd)(60 minute/hour)
PMRg = (PMRc)(Mg/Mcg)
PMR = (PMRg)(#hours)
MMPE FIELD LOG:
CLIENT: Geological Resources Inc.
JOB NAME: Kingsway #10 System B
LOCATION: Gastonia, NC
MMPE EVENT DATES: January 9 - 13, 2023
EXTRACTION POINTS: RW-1 and MW-2
AES JOB NUMBER: 01 - 2301
DATE TIME FLOW (f/m) HUM.(%) TEMP. (F)VOC's(ppm)VAC. (hg")GALLONS STINGER/WL's EXTRACTION POINTS (hg")
RW-2 RW-3
Stinger(ft)28 28
Start 12:00 Initial WL's 28.17 27.72

01/09/23 12:20 3,800 99.0 102 1,400 14.0 10.0 10.0
13:20 3,800 99.0 108 1,400 14.0 10.0 10.0
18:30 3,800 99.0 118 1,100 14.0 10.0 10.0
19:30 3,800 99.0 118 1,100 14.0 10.0 10.0
01/10/23 8:20 3,600 99.0 116 900 15.0 11.0 11.0
10:20 3,600 99.0 118 900 15.0 11.0 11.0
16:00 3,600 99.0 120 900 15.0 11.0 11.0
18:00 3,600 99.0 120 900 15.0 11.0 11.0
01/11/23 8:30 3,600 99.0 118 700 15.0 11.0 11.0
10:30 3,600 99.0 118 700 15.0 11.0 11.0
12:30 3,600 99.0 120 700 15.0 11.0 11.0
17:00 3,600 99.0 120 700 15.0 11.0 11.0
01/12/23 8:20 3,600 99.0 116 600 15.0 11.0 11.0
10:20 3,600 99.0 118 600 15.0 11.0 11.0
12:20 3,600 99.0 118 600 15.0 P/O 510 gal.11.0 11.0
16:40 3,600 99.0 118 600 15.0 11.0 11.0
01/13/23 10:00 3,600 99.0 118 600 15.0 11.0 11.0
11:00 3,600 99.0 118 600 15.0 11.0 11.0
End 12:00 Final WL's 30.28 30.80
Total fluids: 3,685 gal.
Total free product:0 gal.
DATE TIME STINGER/WL's EXTRACTION POINTS (hg") cont. VACUUM INFLUENCE (h2o") WELL GAUGING (ft)
MW-3 MW-9 MW-3 MW-9
Stinger(ft)
Initial WL's
01/09/23 12:20 0.00 0.00 28.04 27.85
13:20
18:30
19:30
01/10/23 8:20
10:20 0.00 5.00+28.19 28.93
16:00
18:00
01/11/23 8:30
10:30
12:30 0.00 5.00+28.31 29.88
17:00
01/12/23 8:20
10:20
12:20 0.00 5.00+28.36 30.10
16:40
01/13/23 10:00
11:00 0.00 5.00+28.42 30.24

End 12:00
Page 1 of 1
MOBILE MULTI-PHASE EXTRACTION EVENT
SITE NAME: Kingsway #10 System B CLIENT: Geological Resources
INCIDENT NUMBER:
AVERAGE DEPTH TO GROUNDWATER: 27 - 29 feet
DESCRIBE SOIL IN THE SATURATED ZONE:
AVERAGE HYDRAULIC CONDUCTIVITY (if known):
EXTRACTION WELLS USED FOR MMPE: RW-2 and RW-3
SPECIFICATIONS OF THE MMPE SYSTEM (cfm @ in Hg): 130 cfm @ 21.0"Hg
DRY STANDARD CUBIC FEET PER MINUTE (DSCFM) AIR FLOW CALCULATIONS (Qstd)
Date Hours Vacuum Velocity Pipe ID Temp Rel Humid Water Water Qstd(inches of Hg)(ft/min)(in)(°F)(%)Vapor (Wt%)Vapor (Vol%)(flow)
1/9/23 24.00 14.00 3600.00 2 112 99.0 0.057 0.084 66
1/10/23 48.00 15.00 3800.00 2 119 99.0 0.080 0.114 67
1/11/23 72.00 15.00 3800.00 2 119 99.0 0.082 0.116 67
1/12/23 96.00 15.00 3800.00 2 118 99.0 0.078 0.111 67
1/13/23
NOTES
Qstd = Flow at DSCFM
Vacuum = The level of vacuum being applied should be recorded from the MMPE system (inches of Hg)
Velocity = The rate at which air flows is measured at the blower discharge piping (anemometer or pitot tube)
Pipe ID = The inside diameter of the blower discharge piping (from the MMPE system)
Temperature = The temperature of the air stream exiting the blower discharge piping (dry bulb temp., in deg.°F)Relative humidity = The % relative humidity of the air stream exiting the blower discharge piping
Bwsw = water vapor % by weight, i.e., pounds of water per pound of dry air, derived from the Psychrometric chart (temp Vs relative humidity)
Bws = water vapor % by volume
EQUATIONS
Bws = (Bwsw/18 lb-mole H20)/[(1/28.84 lb-mole dry air) + (Bwsw/18 lb-mole H2O)]Qstd = (1-Water Vapor) * velocity * (PI * (diameter/24)2) * (528°R/(Temp + 460))
EMISSION CALCULATIONS
Elapsed
Time Flow PPMmeasured PPMwet PPMdry K PPMconc Cc:m Cc PMRc PMRg PMR
(hour)(DSCFM)(ppm)(#C - gas)(mg/dsm3)(lb/dscf)(lb/hour)(lb/hour)(lb)
24 66 1250 1250 1364 1 1364 681 4.24937E-05 0.17 0.20 4.71
48 67 900 900 1015 1 1015 507 3.16286E-05 0.13 0.15 3.54
72 67 700 700 792 1 792 395 2.46699E-05 0.10 0.11 2.75
96 67 600 600 675 1 675 337 2.10259E-05 0.08 0.10 2.36
Total emissions in pounds 13.35
Total emissions as gallons (pounds / 6.152)2.17
NOTES
PPMmeasured = Actual measurements (ppm) taken with a OVA or TVA at the blower discharge piping
PPMwet = "wet" concentration
PPMdry = "dry" concentration
K = Number of carbons in calibration gas: (Methane K = 1, or Propane K = 3, or Hexane K = 6)
PPMc= PPMv, Volumetric concentration of VOC emissions as carbon, dry basis at STP
Cc:m = mg/dsm3, mass concentration of VOC emissions as carbon
Mc = 12.01 mg/mg-mole, molecular weight of carbon
K3 = 24.07 dsm3/106 mg-mole, mass to volume conversion factor at STP
Cc = lb/dcsf, mass concentration of VOC emissions as carbon, dry basis at STP
PMRc = lb/hr, pollutant mass removal rate of VOC's as carbon
PMRg = lb/hr, pollutant mass removal rate of of VOC's as gasolinePMR = lb, pollutant mass removal of VOC's as gasoline
EQUATIONS
PPMwet = PPMmeasuredPPMdry = (PPMwet)/(1-Bws)
PPMc = (PPMd)(K)
Cc:m = (PPMc)(Mc / K3)Cc = (Cc:m)(62.43x10-9 lb-m3/mg-ft3)
PMRc = (Cc)(Qstd)(60 minute/hour)
PMRg = (PMRc)(Mg/Mcg)
PMR = (PMRg)(#hours)
MMPR Pleld Loa
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