WS-96266_96906_CA_IAR_20230209

INITIAL ABATEMENT ACTION REPORT

HOLDEN BROTHERS PROPERTY
715 BAKER ROAD
HIGH POINT, GUILFORD COUNTY, NORTH CAROLINA
GROUNDWATER INCIDENT: 96906 FACILITY ID: N/A FEBRUARY 9, 2023 AST OWNER (NOT OPERATOR): Holden Brothers, LLC 1799 Trier Drive Greensboro, NC 27455 Phone Number: [phone]
PROPERTY OWNER:
Same as UST Owner

CONSULTANT:
Paragon Environmental Consultants, Inc. P. O. Box 157 Thomasville, NC 27361-0157 Phone Number: [phone]

RELEASE INFORMATION:
Date Discovered: January 3, 2023
Estimated Quantity of Release: Unknown
Cause of Release: AST with product inside tipped over during removal
Source of Release: AST
Size and Contents: One (1) 275 Gallon Heating Oil AST
Latitude: N 35.925667o Longitude: W 79.972978o

The Initial Abatement Action Report for this site has been prepared by Paragon
Environmental Consultants, Inc. under the direct supervision of a licensed geologist. All
activities performed on this project were conducted under my direct supervision:
Benjamin W. Robinson, L.G.
North Carolina License #2466

February 9, 2023

Satya Modi Holden Brothers, LLC 1799 Trier Drive Greensboro, NC 27455

Reference: Initial Abatement Action Report
Holden Brothers Property
715 Baker Road
High Point, Guilford County, North Carolina
Groundwater Incident: 96906
Facility ID: Not Applicable

Dear Mr. Modi:

In accordance with the requirements of the current UST Section guidelines, contained
herein is an Initial Abatement Action Report for the release which occurred at the above
referenced facility. These activities have been conducted following the surface release of
petroleum which occurred from one 275 gallon heating oil aboveground storage tank
(AST). The soil remediation consisted of the excavation and disposal of approximately 55
cubic yards of contaminated soil and confirmatory sampling of in-situ soils. All activities
were conducted in accordance with North Carolina Department of Environmental Quality
(NC DEQ) guidelines and the requirements of 15A NCAC 2N.

Mr. Modi, if you have questions regarding this report, please contact our office.
Sincerely,
Benjamin W. Robinson, L.G.
Paragon Environmental Consultants, Inc.

R23-2301
PARAGON
Environmental Consultants, Inc.
P.O. Box 157 • Thomasville, NC 27361-0157
Business Ph: [phone] • Fax: [phone]

TABLE OF CONTENTS

Section Page

B. Site History

1. Introduction .................................................................... 1
2. Scope of Services ........................................................... 1
C. Site Investigation 1. Excavation and Soil Sampling ....................................... 2 2. Soil Disposal .................................................................. 2 3. Conclusions and Recommendations .............................. 3
D. Figures Figure 1: Project Location Figure 2: Site Layout and Former AST Location Figure 3: Remedial Excavation and Soil Sample Locations E. Tables Table 1: Summary of TPH Laboratory Analytical Results Table 2: Summary of “Risk-Based” Soil Analytical Results F. Appendices Appendix A: Geologic Log of Excavation Appendix B: Soil Analytical Results Appendix C: Standard Operating Procedures Appendix D: Soil Disposal Manifests
Page - 1
INITIAL ABATEMENT ACTION REPORT
Holden Brothers Property 715 Baker Road High Point, North Carolina

B. Site History

1. Introduction

Holden Brothers, LLC owns a property located at 715 Baker Road in High Point, NC. This
property contains one permanent structure, which was formerly in use as a residence, but
is currently vacant. Figure 1 illustrates the location of this facility on the High Point East
Quadrangle U.S.G.S. Topographic Map. The site formerly contained one 275 gallon
heating oil AST which was used for heating the residence. Figure 2 illustrates the site
layout and the location of the former AST. A surface release from this 275 gallon tank
occurred when it was removed. The AST still contained fuel while it was moved, causing
it to tip over and spill heating oil onto the surface soils of 715 Baker Road and 717 Baker
Road. The AST was removed before the remediation of the surface soils. Two soil samples
collected from the stockpile of contaminated soil during the remedial excavation were
reported at maximum levels of 26,000 milligrams per kilogram (mg/kg) by Diesel Range
Organics (DRO) and 208 mg/kg by Gasoline Range Organics (GRO).

Following discovery of the surficial contamination, Paragon Environmental Consultants,
Inc. was contracted by Holden Brothers, LLC to perform soil remediation activities and
confirmatory soil sampling and laboratory analyses from the surface soils down-gradient
of the heating oil AST. Contained herein is a summary of activities which were completed
at the project site.

2. Scope of Services
This Initial Abatement Action Report contains documentation concerning the following activities which have been conducted at this facility:

o Excavation of contaminated soils and backfilling of the excavation performed by
L. C. Better Homes, LLC of Archdale, NC

o Transportation of contaminated soil by JEA Transport Corp. and disposal of the
excavated material at AES of NC in Thomasville, NC

o Collection of soil samples from the final vertical limits of the excavation performed
by Paragon Environmental Consultants, Inc.

o Laboratory analyses of soil samples conducted by Waypoint Analytical, LLC of
Charlotte, NC

Page - 2

C. Site Investigation

1. Excavation and Soil Sampling
On January 20, 2023 personnel from L. C. Better Homes, LLC and Paragon Environmental Consultants, Inc. (Paragon) excavated the petroleum impacted soil that resulted from the spill event. The AST was removed from the site prior to January 20, 2023. The impacted soils in the excavation area were excavated until field analyses indicated that all petroleum contaminated soil had been removed. In order to verify site conditions, ten samples were collected from beneath the excavated surface soils at depths ranging between approximately 6 inches to approximately four and a half feet below the original surface grade. Appendix A contains a geologic log of excavation for the soil remediation activities at this facility. The soil samples collected from the remedial excavation at 715 Baker Road and 717 Baker Road were analyzed according to DRO and GRO for Total Petroleum Hydrocarbons (TPH). Soil Sample #4 (SS-4) was also analyzed by EPA Methods 8260 and 8270 as well as MADEP methods for Volatile Petroleum Hydrocarbons (VPH) and Extractable Petroleum Hydrocarbons (EPH). Ten in-situ soil samples were obtained from the bottom of the remedial excavation and two composite stockpiles were obtained from the contaminated material. These samples were obtained with the excavator bucket and were immediately placed into laboratory supplied glassware and placed on ice for transportation to the analytical laboratory utilizing EPA approved chain-of-custody procedures. According to the laboratory analytical results, Soil Sample #4 was reported at a concentration of 131 mg/kg by DRO, which exceeds the NCDEQ action level of 100 mg/kg. The remaining nine in-situ samples, labeled as Soil Sample #1 (SS-1) through Soil Sample #3 (SS-3) and Soil Sample #5 (SS-5) through Soil Sample #10 (SS-10), were below the NCDEQ action levels for TPH by DRO and GRO. Soil Sample #4 (SS-4) was below the lowest Maximum Soil Contaminant Concentrations (MSCCs) by EPA Methods 8260 and 8270, as well as the carbon fraction classes by VPH and EPH. Based on the soil sample results from the limits of the remedial excavation, no contamination above the applicable soil standards remains at 715 Baker Road and 717 Baker Road. Figure 3 illustrates the area of soil remediation and the locations of the soil samples
collected at 715 Baker Road and 717 Baker Road. The analytical results for the TPH soil
analyses are summarized in Table 1. Table 2 contains a summary of the “Risk-Based” soil
sample results. A copy of the laboratory analytical report and the chain-of-custody record
for the samples from 715 Baker Road and 717 Baker Road is included in Appendix B. All
samples were obtained in accordance with Paragon’s Standard Operating Procedures which
are included as Appendix C.

2. Soil Disposal

A total of approximately 55 cubic yards (77.50 tons) of heating oil impacted soils were removed during site remediation activities on January 20, 2023. This material was transported by JEA Transport Corp. to AES of NC’s facility in Thomasville, NC for treatment and disposal. Copies of the soil disposal manifests are contained as Appendix D.
Page - 3
3. Conclusions and Recommendations
3. A Conclusions and Recommendations

The soil remediation activities at the Holden Brothers Property have been completed. From a review of all information gathered during this removal project, Paragon Environmental Consultants, Inc. makes the following conclusions:

o Laboratory results for sampling of in-situ soils following the excavation activities showed Soil Sample #4 with a DRO level of 131 mg/kg. The other nine samples were below the action limits for TPH according to DRO and GRO.
o The Soil Sample #4 was below the lowest MSCCs according to EPA Methods 8260 and 8270 as well as for MADEP methods for VPH and EPH.

o A total of 77.50 tons of heating oil impacted soils were removed from the area of
the surface release. This material was transported by JEA Transport Corp. to AES
of NC’s facility in Thomasville, NC for disposal.

3. B. Recommendations
Based upon a review of all information gathered during this Initial Abatement project, Paragon makes the following recommendations:
o Since the laboratory analytical results for the in-situ soil samples confirm that all petroleum impacted soil due to the AST spill has been removed from 715 Baker Road and 717 Baker Road, Paragon recommends that a Notice of No Further Action be issued for the incident at the Holden Brothers Property.

o A copy of this report should be forwarded to the following address:

Guilford County Health Department
400 W. Market Street – Suite 300
Greensboro, NC 27401

3. C. Limitations
This report has been prepared for the exclusive use of Holden Brothers, LLC for the specific application to the referenced site located in Guilford County, North Carolina. The assessment was conducted based on the scope of work and level of effort desired by the client. Our findings have been developed in accordance with generally accepted standards in the practice of Initial Abatement Action Reports in the State of North Carolina, available information, and our professional judgment. No other warranty is expressed or implied.
The data presented in this report are indicative of conditions that existed at the precise locations sampled and at the time the samples were collected. Additionally, the data obtained from the samples would be interpreted as meaningful with respect to the parameters indicated in the laboratory reports. No additional information can be logically inferred from this data.

FIGURES

TABLES

TABLE 1
SUMMARY OF TPH LABORATORY ANALYTICAL RESULTS

Holden Brothers Property
High Point, North Carolina

SAMPLE LOCATION DATE DEPTH TPH by DRO* TPH by GRO* OVA
ID (FT)

X-1 Stockpile #1 1/20/23 N/A 17,200 208 N/A
X-2 Stockpile #2 1/20/23 N/A 26,000 189 N/A
SS-1 Soil Sample #1 1/20/23 3.5' 14.2 <10 N/A
SS-2 Soil Sample #2 1/20/23 4.5' 14 <10 N/A
SS-3 Soil Sample #3 1/20/23 2' 10.5 <10 N/A
SS-4 Soil Sample #4 1/20/23 2.5' 131 <10 N/A
SS-5 Soil Sample #5 1/20/23 1.5' 88.5 <10 N/A
SS-6 Soil Sample #6 1/20/23 1’ 17.2 <10 N/A
SS-7 Soil Sample #7 1/20/23 1' 9.05 <10 N/A
SS-8 Soil Sample #8 1/20/23 1' 16.2 20.3 N/A
SS-9 Soil Sample #9 1/20/23 0.5' 7.54 <10 N/A
SS-10 Soil Sample #10 1/20/23 0.5' 22.6 <10 N/A

* Results in milligrams per kilogram (mg/kg)

<10 = Below Detection Limits
N/A = Not Analyzed

R23-2301T
TABLE 2
Summary of "Risk-Based" Soil Analytical Results
Holden Brorthers Property
High Point, North Carolina
Constituent SS-4 Lowest MSCCs Residential Standards
Date 1/20/2023
Method 8260 (mg/kg)
Acetone 0.024 24 14,000
Benzene BDL 0.0072 12
n-Butylbenzene BDL 2.4 782
sec-Butylbenzene BDL 2.2 1,560
Carbon Disulfide BDL 3.7 1,560
Di-Isopropyl Ether (DIPE)BDL 0.32 NSE
Ethylbenzene BDL 8 60.3
n-Hexane BDL NSE NSE
Isopropylbenzene BDL 1.3 1,560
p-Isopropyltoluene BDL 0.12 1,560
Methyl Tert Butyl Ether (MTBE)BDL 0.085 156
Methylene Chloride BDL 0.023 93.8
Naphthalene BDL 0.2 5.5
n-Propylbenzene BDL 1.4 1,560.0
Toluene BDL 5.4 1,250
1,2,4-Trimethylbenzene BDL 6.6 156
1,3,5-Trimethylbenzene BDL 6.6 156
Xylenes (total)BDL 6 3,120
Method 8270 (mg/kg)
Chrysene BDL 18 663
Fluoranthene BDL 330 625
2-Ethylhexyl Phthalate 1.71 6.6 47
Naphthalene BDL 0.2 5.5
Phenanthrene BDL 64 469
Pyrene BDL 210 469
Aliphatic Fraction Classes (mg/kg)
C5-C8 Volatile Aliphatics BDL 68 625
C9-C12 Volatile Aliphatics BDL NSE NSE
C9-C18 Extractable Aliphatics BDL NSE NSE
C9-C18 Aliphatics (total)BDL 540 1,560
C19-C36 Extractable Aliphatics BDL NSE 31,200
Aromatic Fraction Classes (mg/kg)
C9-C10 Volatile Aromatics BDL NSE NSE
C11-C22 Extractable Aromatics BDL NSE NSE
C9-C22 Aromatics (total)BDL 31 469
BDL= Below Detection Limits
NSE = No Standard Established X23-2301

APPENDIX A

GEOLOGIC LOG OF EXCAVATION

GEOLOGIC LOG OF EXCAVATION
Paragon Environmental Consultants, Inc.
Job Name:Holden Brothers Property
Address:715 Baker Road and 717 Baker Road High Point, NC 27263
Job No.:P-2301 Excavation Method:Excavator
Start Date:1/20/23 Sample Method:Excavator Bucket
Contractor:L. C. Better Homes, LLC Sampled By:BWR
Sample ID:Soil Remediation Samples Logged By:BWR
Comments:

Sample Depth OVA
Number (FT.)Soil Decription (color, soil type, moisture) (ppm)
SS-1 3.5 Tan/brown, CLAY with silt, damp N/A
SS-2 4.5 Tan/brown, CLAY with silt, damp N/A
SS-3 2 Tan, CLAY with silt, damp N/A
SS-4 2.5 Red/brown, SILT with clay, damp N/A
SS-5 1.5 Brown, SILT with clay, damp N/A
SS-6 1 Brown/red, SILT with clay, damp N/A
SS-7 1 Dark Brown, SILT with clay, damp N/A
SS-8 1 Dark Brown, SILT with clay, damp N/A
SS-9 0.5 Dark Brown, SILT with clay, damp N/A
SS-10 0.5 Dark Brown, SILT with clay, damp N/A
P-2301X

APPENDIX B

SOIL ANALYTICAL RESULTS

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

1/31/2023
Paragon Environmental Consultants, Inc. Brandon Moore
PO Box 157 Thomasville, NC, 27361
Ref: Analytical Testing
Lab Report Number: 23-023-0016 Client Project Description: Holden Brothers Property
P-2301
Dear Brandon Moore:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/23/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 37
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-023-0016
Page 2 of 37
Report Number:
Sample Summary Table
Client Project Description:
23-023-0016
Holden Brothers Property
P-2301
Lab No Client Sample ID Matrix Date Collected Date Received
01/20/2023 09:00Solids 98202 X-1 01/23/2023 14:58
01/20/2023 14:00Solids 98203 X-2 01/23/2023 14:58
01/20/2023 15:00Solids 98204 SS-1 01/23/2023 14:58
01/20/2023 15:10Solids 98205 SS-2 01/23/2023 14:58
01/20/2023 15:20Solids 98206 SS-3 01/23/2023 14:58
01/20/2023 15:30Solids 98207 SS-4 01/23/2023 14:58
01/20/2023 15:40Solids 98208 SS-5 01/23/2023 14:58
01/20/2023 15:50Solids 98209 SS-6 01/23/2023 14:58
01/20/2023 16:00Solids 98210 SS-7 01/23/2023 14:58
01/20/2023 16:10Solids 98211 SS-8 01/23/2023 14:58
01/20/2023 16:20Solids 98212 SS-9 01/23/2023 14:58
01/20/2023 16:30Solids 98213 SS-10 01/23/2023 14:58
Page 3 of 37
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-023-0016
Report Limit
Project:Holden Brothers Property
V 98202X-1
B1720001/30/2023 10:548015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 822
208 01/24/2023 21:088015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 3.82
43.4 01/24/2023 16:21SW-DRYWT Moisture %
V 98203X-2
B2600001/30/2023 11:158015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 770
189 01/24/2023 20:398015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 3.43
39.6 01/24/2023 16:21SW-DRYWT Moisture %
V 98204SS-1
14.2 01/31/2023 10:288015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.95
21.9 01/24/2023 16:21SW-DRYWT Moisture %
V 98205SS-2
14.0 01/31/2023 10:498015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.92
21.5 01/24/2023 16:21SW-DRYWT Moisture %
V 98206SS-3
J10.5 01/31/2023 11:108015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 6.09
23.6 01/24/2023 16:21SW-DRYWT Moisture %
V 98207SS-4
131 01/31/2023 11:318015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 6.64
30.0 01/24/2023 16:21SW-DRYWT Moisture %
V 98208SS-5
88.5 01/31/2023 11:528015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 6.52
28.7 01/24/2023 16:21SW-DRYWT Moisture %
V 98209SS-6
17.2 01/31/2023 12:138015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.81
19.9 01/24/2023 16:21SW-DRYWT Moisture %
V 98210SS-7
J9.05 01/31/2023 12:358015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.40
13.9 01/24/2023 16:21SW-DRYWT Moisture %
V 98211SS-8
16.2 01/31/2023 12:568015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.53
20.3 01/24/2023 18:458015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.46
Page 4 of 37
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-023-0016
Report Limit
Project:Holden Brothers Property
V 98211SS-8
15.9 01/24/2023 16:21SW-DRYWT Moisture %
V 98212SS-9
J7.54 01/31/2023 13:178015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.81
20.0 01/24/2023 16:21SW-DRYWT Moisture %
V 98213SS-10
22.6 01/31/2023 13:388015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.54
16.0 01/24/2023 16:21SW-DRYWT Moisture %
Page 5 of 37

Client: Paragon Environmental Consultants, Inc. CASE NARRATIVE
Project: Holden Brothers Property Lab Report Number: 23-023-0016
Date: 1/31/2023
Total Petroleum Hydrocarbons - Extractable Method 8015C DRO QC Batch No: V29311/V29211 Target analyte(s) was identified in the method blank associated with this project, below the Method Quantitation
Limit. Per laboratory protocol any associated affected sample result is flagged "B" to indicate that it was detected in the method blank.
Sample 98203 (X-2)
QC Batch No: V29311/V29211 Method Blank shows a J flag result. Sample result is 10x higher than Method blank result. The validity of the
data is unaffected.
Sample 98202 (X-1) Analyte: Diesel Range Organics (C10-C28)
QC Batch No: V29311/V29211 Method Blank shows a J flag result. Sample result is 10x higher than Method blank result. The validity of the
data is unaffected.
Sample 98202 (X-1) Analyte: Diesel Range Organics (C10-C28)
QC Batch No: V29311/V29211 Sample requires dilution due to high levels of target and/or non-target analytes. Sample 98203 (X-2)
Analyte: Diesel Range Organics (C10-C28) QC Batch No: V29311/V29211
Sample requires dilution due to high levels of target and/or non-target analytes.
Sample 98202 (X-1) Analyte: o-Terphenyl QC Batch No: V29311/V29211 Surrogate(s) flagged for recovery outside QC limits in this project sample due to a required dilution. The dilution
factor resulted in surrogate concentration(s) below the minimum detectable level. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Sample 98203 (X-2) Analyte: o-Terphenyl QC Batch No: V29311/V29211 Surrogate(s) flagged for recovery outside QC limits in this project sample due to a required dilution. The dilution factor resulted in surrogate concentration(s) below the minimum detectable level. Batch QC samples (method
blank and laboratory control samples) all showed surrogates within QC limits.
Page 6 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:X-1
98202 Matrix:
1/20/2023 9:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
43.4 %Moisture 1 01/24/23 16:21 SW-DRYWTAMB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 7 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:X-1
98202 Matrix:
1/20/2023 9:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V29211 01/27/23 13:30
17200 B mg/Kg - dry 822 1770Diesel Range Organics (C10-C28)100 01/30/23 10:54 V29311AMP
8015C DROSurrogate: OTP Surrogate 0 *Limits: 31-123%01/30/23 10:54100 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V29129 01/24/23 08:00
208 mg/Kg - dry 3.82 9.20Gasoline Range Organics (C6-C10)50 01/24/23 21:08 V29130TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 108 Limits: 50-137%01/24/23 21:0850 TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 8 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:X-2
98203 Matrix:
1/20/2023 14:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
39.6 %Moisture 1 01/24/23 16:21 SW-DRYWTAMB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 9 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:X-2
98203 Matrix:
1/20/2023 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V29211 01/27/23 13:30
26000 B mg/Kg - dry 770 1660Diesel Range Organics (C10-C28)100 01/30/23 11:15 V29311AMP
8015C DROSurrogate: OTP Surrogate 0 *Limits: 31-123%01/30/23 11:15100 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V29129 01/24/23 08:00
189 mg/Kg - dry 3.43 8.28Gasoline Range Organics (C6-C10)50 01/24/23 20:39 V29130TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 110 Limits: 50-137%01/24/23 20:3950 TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 10 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-1
98204 Matrix:
1/20/2023 15:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.9 %Moisture 1 01/24/23 16:21 SW-DRYWTAMB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 11 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-1
98204 Matrix:
1/20/2023 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V29312 01/30/23 13:50
14.2 mg/Kg - dry 5.95 12.8Diesel Range Organics (C10-C28)1 01/31/23 10:28 V29317AMP
8015C DROSurrogate: OTP Surrogate 67.6 Limits: 31-123%01/31/23 10:281 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V29129 01/24/23 08:00
<2.69 mg/Kg - dry 2.69 6.50Gasoline Range Organics (C6-C10)50 01/24/23 15:27 V29130TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 118 Limits: 50-137%01/24/23 15:2750 TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 12 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-2
98205 Matrix:
1/20/2023 15:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.5 %Moisture 1 01/24/23 16:21 SW-DRYWTAMB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-2
98205 Matrix:
1/20/2023 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V29312 01/30/23 13:50
14.0 mg/Kg - dry 5.92 12.7Diesel Range Organics (C10-C28)1 01/31/23 10:49 V29317AMP
8015C DROSurrogate: OTP Surrogate 73.6 Limits: 31-123%01/31/23 10:491 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V29129 01/24/23 08:00
<2.64 mg/Kg - dry 2.64 6.37Gasoline Range Organics (C6-C10)50 01/24/23 15:55 V29130TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 117 Limits: 50-137%01/24/23 15:5550 TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-3
98206 Matrix:
1/20/2023 15:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.6 %Moisture 1 01/24/23 16:21 SW-DRYWTAMB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-3
98206 Matrix:
1/20/2023 15:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V29312 01/30/23 13:50
10.5 J mg/Kg - dry 6.09 13.1Diesel Range Organics (C10-C28)1 01/31/23 11:10 V29317AMP
8015C DROSurrogate: OTP Surrogate 67.5 Limits: 31-123%01/31/23 11:101 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V29129 01/24/23 08:00
<2.71 mg/Kg - dry 2.71 6.54Gasoline Range Organics (C6-C10)50 01/24/23 16:23 V29130TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 119 Limits: 50-137%01/24/23 16:2350 TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 16 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-4
98207 Matrix:
1/20/2023 15:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
30.0 %Moisture 1 01/24/23 16:21 SW-DRYWTAMB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 17 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-4
98207 Matrix:
1/20/2023 15:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V29312 01/30/23 13:50
131 mg/Kg - dry 6.64 14.3Diesel Range Organics (C10-C28)1 01/31/23 11:31 V29317AMP
8015C DROSurrogate: OTP Surrogate 82.0 Limits: 31-123%01/31/23 11:311 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V29129 01/24/23 08:00
<2.96 mg/Kg - dry 2.96 7.14Gasoline Range Organics (C6-C10)50 01/24/23 16:52 V29130TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 93.4 Limits: 50-137%01/24/23 16:5250 TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-5
98208 Matrix:
1/20/2023 15:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
28.7 %Moisture 1 01/24/23 16:21 SW-DRYWTAMB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-5
98208 Matrix:
1/20/2023 15:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V29312 01/30/23 13:50
88.5 mg/Kg - dry 6.52 14.0Diesel Range Organics (C10-C28)1 01/31/23 11:52 V29317AMP
8015C DROSurrogate: OTP Surrogate 69.7 Limits: 31-123%01/31/23 11:521 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V29129 01/24/23 08:00
<3.28 mg/Kg - dry 3.28 7.94Gasoline Range Organics (C6-C10)50 01/24/23 17:20 V29130TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 107 Limits: 50-137%01/24/23 17:2050 TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 20 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-6
98209 Matrix:
1/20/2023 15:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.9 %Moisture 1 01/24/23 16:21 SW-DRYWTAMB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 21 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-6
98209 Matrix:
1/20/2023 15:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V29312 01/30/23 13:50
17.2 mg/Kg - dry 5.81 12.5Diesel Range Organics (C10-C28)1 01/31/23 12:13 V29317AMP
8015C DROSurrogate: OTP Surrogate 59.8 Limits: 31-123%01/31/23 12:131 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V29129 01/24/23 08:00
<2.58 mg/Kg - dry 2.58 6.24Gasoline Range Organics (C6-C10)50 01/24/23 17:49 V29130TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 132 Limits: 50-137%01/24/23 17:4950 TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 22 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-7
98210 Matrix:
1/20/2023 16:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.9 %Moisture 1 01/24/23 16:21 SW-DRYWTAMB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 23 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-7
98210 Matrix:
1/20/2023 16:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V29312 01/30/23 13:50
9.05 J mg/Kg - dry 5.40 11.6Diesel Range Organics (C10-C28)1 01/31/23 12:35 V29317AMP
8015C DROSurrogate: OTP Surrogate 69.6 Limits: 31-123%01/31/23 12:351 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V29129 01/24/23 08:00
<2.40 mg/Kg - dry 2.40 5.81Gasoline Range Organics (C6-C10)50 01/24/23 18:18 V29130TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 120 Limits: 50-137%01/24/23 18:1850 TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 24 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-8
98211 Matrix:
1/20/2023 16:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
15.9 %Moisture 1 01/24/23 16:21 SW-DRYWTAMB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 25 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-8
98211 Matrix:
1/20/2023 16:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V29312 01/30/23 13:50
16.2 mg/Kg - dry 5.53 11.9Diesel Range Organics (C10-C28)1 01/31/23 12:56 V29317AMP
8015C DROSurrogate: OTP Surrogate 75.2 Limits: 31-123%01/31/23 12:561 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V29129 01/24/23 08:00
20.3 mg/Kg - dry 2.46 5.95Gasoline Range Organics (C6-C10)50 01/24/23 18:45 V29130TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 127 Limits: 50-137%01/24/23 18:4550 TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 26 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-9
98212 Matrix:
1/20/2023 16:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.0 %Moisture 1 01/24/23 16:21 SW-DRYWTAMB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 27 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-9
98212 Matrix:
1/20/2023 16:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V29312 01/30/23 13:50
7.54 J mg/Kg - dry 5.81 12.5Diesel Range Organics (C10-C28)1 01/31/23 13:17 V29317AMP
8015C DROSurrogate: OTP Surrogate 68.6 Limits: 31-123%01/31/23 13:171 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V29129 01/24/23 08:00
<2.59 mg/Kg - dry 2.59 6.25Gasoline Range Organics (C6-C10)50 01/24/23 19:14 V29130TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 113 Limits: 50-137%01/24/23 19:1450 TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 28 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-10
98213 Matrix:
1/20/2023 16:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.0 %Moisture 1 01/24/23 16:21 SW-DRYWTAMB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 29 of 37
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-023-0016
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 01/23/2023
Holden Brothers Property
Report Date : 01/31/2023
Sample ID :
Lab No :
Sampled:SS-10
98213 Matrix:
1/20/2023 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V29312 01/30/23 13:50
22.6 mg/Kg - dry 5.54 11.9Diesel Range Organics (C10-C28)1 01/31/23 13:38 V29317AMP
8015C DROSurrogate: OTP Surrogate 78.9 Limits: 31-123%01/31/23 13:381 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V29129 01/24/23 08:00
<2.46 mg/Kg - dry 2.46 5.95Gasoline Range Organics (C6-C10)50 01/24/23 19:42 V29130TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 106 Limits: 50-137%01/24/23 19:4250 TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 30 of 37
Quality Control Data
23-023-0016Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Extractable
8015C DRO
V29311QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29211
Associated Lab Samples: 98202, 98203
LRB-V29211 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/30/23 10:3310.04.655.41mg/KgDiesel Range Organics (C10-C28)
01/30/23 10:33OTP Surrogate (S)77.4 31-123
LCS-V29211Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
11275.066.7mg/KgDiesel Range Organics (C10-C28)46-126
82.7OTP Surrogate (S)31-123
V 98202-MS-V29211 V 98202-MSD-V29211Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
7820 -2700*731066.766.79730mg/KgDiesel Range Organics (C10-C28)-3600*50-117 6.7 24
I*OTP Surrogate (S)I*31-123
Page 1 of 4* QC Fail Date:01/31/2023 03:53 PM
Page 31 of 37
Quality Control Data
23-023-0016Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Extractable
8015C DRO
V29317QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29312
Associated Lab Samples: 98204, 98205, 98206, 98207, 98208, 98209, 98210, 98211, 98212, 98213
LRB-V29312 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/31/23 09:2410.04.65<4.65mg/KgDiesel Range Organics (C10-C28)
01/31/23 09:24OTP Surrogate (S)72.9 31-123
LCS-V29312 LCSD-V29312Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
76.0 11411275.066.7mg/KgDiesel Range Organics (C10-C28)46-126 1.3 20
78.181.2OTP Surrogate (S)31-123
Page 2 of 4Date:01/31/2023 03:53 PM
Page 32 of 37
Quality Control Data
23-023-0016Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Volatile
8015C GRO
V29130QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V29129
Associated Lab Samples: 98202, 98203, 98204, 98205, 98206, 98207, 98208, 98209, 98210, 98211, 98212, 98213
LRB-V29129 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/24/23 14:585.002.07<2.07mg/KgGasoline Range Organics (C6-C10)
01/24/23 14:58a,a,a-Trifluorotoluene (S)113 50-137
LCS-V29129Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
12864.150.0mg/KgGasoline Range Organics (C6-C10)41-138
98.0a,a,a-Trifluorotoluene (S)50-137
V 98204-MS-V29129 V 98204-MSD-V29129Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
48.0 96.046.050.050.0<2.07mg/KgGasoline Range Organics (C6-C10)92.0 41-138 4.2 34
124a,a,a-Trifluorotoluene (S)118 50-137
Page 3 of 4Date:01/31/2023 03:53 PM
Page 33 of 37
Quality Control Data
23-023-0016Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
Dry Weight Determination
SW-DRYWT
V29131QC Analytical Batch:
Analysis Method:
Analysis Description:
V 98202-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 01/24/23 16:214.241.643.4%Moisture
V 98208-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 01/24/23 16:211.728.228.7%Moisture
Page 4 of 4Date:01/31/2023 03:53 PM
Page 34 of 37
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-023-0016
Paragon Environmental Consultants, Inc.
01156
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 2.6C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:01/23/2023 16:58:44
Special precautions or instructions included?
Comments:
Page 35 of 37
Page 36 of 37
Page 37 of 37

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

2/8/2023
Paragon Environmental Consultants, Inc. Brandon Moore
PO Box 157 Thomasville, NC, 27361
Ref: Analytical Testing
Lab Report Number: 23-032-0031 Client Project Description: Holden Brothers Property
P-2301
Dear Brandon Moore:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 2/1/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 31
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-032-0031
Page 2 of 31
Report Number:
Sample Summary Table
Client Project Description:
23-032-0031
Holden Brothers Property
P-2301
Lab No Client Sample ID Matrix Date Collected Date Received
01/20/2023 15:30Solids 98861 SS-4 02/01/2023 14:58
Page 3 of 31
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-032-0031
Report Limit
Project:Holden Brothers Property
V 98861SS-4
J0.024 02/03/2023 11:118260DAcetonemg/Kg - dry 0.002
1.71 02/03/2023 11:158270EBis(2-ethylhexyl)phthalate mg/Kg - dry 0.146
18.3 02/02/2023 11:30SW-DRYWT Moisture %
Page 4 of 31

Client: Paragon Environmental Consultants, Inc. CASE NARRATIVE
Project: Holden Brothers Property Lab Report Number: 23-032-0031
Date: 2/8/2023
Volatile Organic Compounds - GC/MS Method 8260D Analyte: Acrolein QC Batch No: V29482/V29481
Low recovery in LCSD. All other QC passes limits. A standard at or below the RL was run and saw recovery. Analyte not detected in samples. No further action taken.
Semivolatile Organic Compounds - GC/MS Method 8270E
Analyte: Benzoic Acid QC Batch No: V29494/V29430
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.

Page 5 of 31
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-032-0031
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 02/01/2023
Holden Brothers Property
Report Date : 02/08/2023
Sample ID :
Lab No :
Sampled:SS-4
98861 Matrix:
1/20/2023 15:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.3 %Moisture 1 02/02/23 11:30 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 6 of 31
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-032-0031
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 02/01/2023
Holden Brothers Property
Report Date : 02/08/2023
Sample ID :
Lab No :
Sampled:SS-4
98861 Matrix:
1/20/2023 15:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29481 02/03/23 08:00
0.024 J mg/Kg - dry 0.002 0.024Acetone 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 02/03/23 11:11 V29482TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 02/03/23 11:11 V29482TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 02/03/23 11:11 V29482TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 02/03/23 11:11 V29482TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 02/03/23 11:11 V29482TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 02/03/23 11:11 V29482TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 02/03/23 11:11 V29482TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 02/03/23 11:11 V29482TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 02/03/23 11:11 V29482TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 02/03/23 11:11 V29482TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 02/03/23 11:11 V29482TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 02/03/23 11:11 V29482TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 02/03/23 11:11 V29482TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 02/03/23 11:11 V29482TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 02/03/23 11:11 V29482TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 31
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-032-0031
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 02/01/2023
Holden Brothers Property
Report Date : 02/08/2023
Sample ID :
Lab No :
Sampled:SS-4
98861 Matrix:
1/20/2023 15:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29481 02/03/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 02/03/23 11:11 V29482TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 02/03/23 11:11 V29482TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 02/03/23 11:11 V29482TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 02/03/23 11:11 V29482TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 02/03/23 11:11 V29482TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 02/03/23 11:11 V29482TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 02/03/23 11:11 V29482TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 02/03/23 11:11 V29482TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 02/03/23 11:11 V29482TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 02/03/23 11:11 V29482TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 02/03/23 11:11 V29482TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 02/03/23 11:11 V29482TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 02/03/23 11:11 V29482TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 02/03/23 11:11 V29482TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 02/03/23 11:11 V29482TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 02/03/23 11:11 V29482TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 31
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-032-0031
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 02/01/2023
Holden Brothers Property
Report Date : 02/08/2023
Sample ID :
Lab No :
Sampled:SS-4
98861 Matrix:
1/20/2023 15:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29481 02/03/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 02/03/23 11:11 V29482TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 02/03/23 11:11 V29482TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 02/03/23 11:11 V29482TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 02/03/23 11:11 V29482TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 02/03/23 11:11 V29482TBL
<0.0007 mg/Kg - dry 0.0007 0.006
n-Propylbenzene 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 02/03/23 11:11 V29482TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 02/03/23 11:11 V29482TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 02/03/23 11:11 V29482TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 02/03/23 11:11 V29482TBL
<0.0008 mg/Kg - dry 0.0008 0.012
1,2,4-Trichlorobenzene 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 02/03/23 11:11 V29482TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 02/03/23 11:11 V29482TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 02/03/23 11:11 V29482TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 02/03/23 11:11 V29482TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 02/03/23 11:11 V29482TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 31
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-032-0031
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 02/01/2023
Holden Brothers Property
Report Date : 02/08/2023
Sample ID :
Lab No :
Sampled:SS-4
98861 Matrix:
1/20/2023 15:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29481 02/03/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 02/03/23 11:11 V29482TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 02/03/23 11:11 V29482TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 02/03/23 11:11 V29482TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 02/03/23 11:11 V29482TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 02/03/23 11:11 V29482TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 02/03/23 11:11 V29482
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%02/03/23 11:111 TBL V29482
Surrogate: Dibromofluoromethane 103 Limits: 84-123%02/03/23 11:111 TBL V29482
Surrogate: Toluene-d8 95.1 Limits: 76-129%02/03/23 11:111 TBL V29482
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V29430 02/02/23 12:10
<0.141 mg/Kg - dry 0.141 0.809Acenaphthene 1 02/03/23 11:15 V29494JMV
<0.128 mg/Kg - dry 0.128 0.809Acenaphthylene 1 02/03/23 11:15 V29494JMV
<0.186 mg/Kg - dry 0.186 0.809Aniline 1 02/03/23 11:15 V29494JMV
<0.175 mg/Kg - dry 0.175 0.809Anthracene 1 02/03/23 11:15 V29494JMV
<0.170 mg/Kg - dry 0.170 0.809Benzo(a)anthracene 1 02/03/23 11:15 V29494JMV
<0.179 mg/Kg - dry 0.179 0.809
Benzo(a)pyrene 1 02/03/23 11:15 V29494JMV
<0.178 mg/Kg - dry 0.178 0.809Benzo(b)fluoranthene 1 02/03/23 11:15 V29494JMV
<0.166 mg/Kg - dry 0.166 0.809Benzo(g,h,i)perylene 1 02/03/23 11:15 V29494JMV
<0.167 mg/Kg - dry 0.167 0.809Benzo(k)fluoranthene 1 02/03/23 11:15 V29494JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 31
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-032-0031
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 02/01/2023
Holden Brothers Property
Report Date : 02/08/2023
Sample ID :
Lab No :
Sampled:SS-4
98861 Matrix:
1/20/2023 15:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V29430 02/02/23 12:10
<0.709 mg/Kg - dry 0.709 2.45Benzoic Acid 1 02/03/23 11:15 V29494JMV
<0.128 mg/Kg - dry 0.128 0.809Benzyl alcohol 1 02/03/23 11:15 V29494JMV
<0.144 mg/Kg - dry 0.144 0.809Bis(2-Chloroethoxy)methane 1 02/03/23 11:15 V29494JMV
<0.130 mg/Kg - dry 0.130 0.809Bis(2-Chloroethyl)ether 1 02/03/23 11:15 V29494JMV
<0.166 mg/Kg - dry 0.166 0.403Bis(2-Chloroisopropyl)ether 1 02/03/23 11:15 V29494JMV
1.71 mg/Kg - dry 0.146 0.809Bis(2-ethylhexyl)phthalate 1 02/03/23 11:15 V29494JMV
<0.133 mg/Kg - dry 0.133 0.8094-Bromophenyl phenyl ether 1 02/03/23 11:15 V29494JMV
<0.138 mg/Kg - dry 0.138 0.403Butyl benzyl phthalate 1 02/03/23 11:15 V29494JMV
<0.113 mg/Kg - dry 0.113 0.809
4-Chloro-3-methylphenol 1 02/03/23 11:15 V29494JMV
<0.137 mg/Kg - dry 0.137 0.4034-Chloroaniline 1 02/03/23 11:15 V29494JMV
<0.141 mg/Kg - dry 0.141 0.8092-Chloronaphthalene 1 02/03/23 11:15 V29494JMV
<0.120 mg/Kg - dry 0.120 0.8092-Chlorophenol 1 02/03/23 11:15 V29494JMV
<0.154 mg/Kg - dry 0.154 1.224-Chlorophenyl phenyl ether 1 02/03/23 11:15 V29494JMV
<0.173 mg/Kg - dry 0.173 0.809Chrysene 1 02/03/23 11:15 V29494JMV
<0.281 mg/Kg - dry 0.281 0.809Dibenz(a,h)anthracene 1 02/03/23 11:15 V29494JMV
<0.145 mg/Kg - dry 0.145 0.809
Dibenzofuran 1 02/03/23 11:15 V29494JMV
<0.115 mg/Kg - dry 0.115 0.8091,2-Dichlorobenzene 1 02/03/23 11:15 V29494JMV
<0.119 mg/Kg - dry 0.119 0.8091,3-Dichlorobenzene 1 02/03/23 11:15 V29494JMV
<0.119 mg/Kg - dry 0.119 0.4031,4-Dichlorobenzene 1 02/03/23 11:15 V29494JMV
<0.179 mg/Kg - dry 0.179 0.8093,3'-Dichlorobenzidine 1 02/03/23 11:15 V29494JMV
<0.117 mg/Kg - dry 0.117 0.8092,4-Dichlorophenol 1 02/03/23 11:15 V29494JMV
<0.220 mg/Kg - dry 0.220 0.809Diethyl phthalate 1 02/03/23 11:15 V29494JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 31
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-032-0031
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 02/01/2023
Holden Brothers Property
Report Date : 02/08/2023
Sample ID :
Lab No :
Sampled:SS-4
98861 Matrix:
1/20/2023 15:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V29430 02/02/23 12:10
<0.212 mg/Kg - dry 0.212 0.809Dimethyl phthalate 1 02/03/23 11:15 V29494JMV
<0.132 mg/Kg - dry 0.132 0.4032,4-Dimethylphenol 1 02/03/23 11:15 V29494JMV
<0.130 mg/Kg - dry 0.130 0.809Di-n-butyl phthalate 1 02/03/23 11:15 V29494JMV
<0.293 mg/Kg - dry 0.293 1.844,6-Dinitro-2-methylphenol 1 02/03/23 11:15 V29494JMV
<0.636 mg/Kg - dry 0.636 1.842,4-Dinitrophenol 1 02/03/23 11:15 V29494JMV
<0.118 mg/Kg - dry 0.118 0.8092,4-Dinitrotoluene 1 02/03/23 11:15 V29494JMV
<0.132 mg/Kg - dry 0.132 0.8092,6-Dinitrotoluene 1 02/03/23 11:15 V29494JMV
<0.175 mg/Kg - dry 0.175 0.403Di-n-Octyl Phthalate 1 02/03/23 11:15 V29494JMV
<0.150 mg/Kg - dry 0.150 0.809
Fluoranthene 1 02/03/23 11:15 V29494JMV
<0.156 mg/Kg - dry 0.156 0.809Fluorene 1 02/03/23 11:15 V29494JMV
<0.129 mg/Kg - dry 0.129 0.809Hexachlorobenzene 1 02/03/23 11:15 V29494JMV
<0.119 mg/Kg - dry 0.119 0.809Hexachlorobutadiene 1 02/03/23 11:15 V29494JMV
<0.192 mg/Kg - dry 0.192 0.809Hexachlorocyclopentadiene 1 02/03/23 11:15 V29494JMV
<0.097 mg/Kg - dry 0.097 0.809Hexachloroethane 1 02/03/23 11:15 V29494JMV
<0.219 mg/Kg - dry 0.219 0.809Indeno(1,2,3-cd)pyrene 1 02/03/23 11:15 V29494JMV
<0.233 mg/Kg - dry 0.233 0.809
Isophorone 1 02/03/23 11:15 V29494JMV
<0.129 mg/Kg - dry 0.129 0.8091-Methylnaphthalene 1 02/03/23 11:15 V29494JMV
<0.122 mg/Kg - dry 0.122 0.8092-Methylnaphthalene 1 02/03/23 11:15 V29494JMV
<0.118 mg/Kg - dry 0.118 0.8092-Methylphenol 1 02/03/23 11:15 V29494JMV
<0.104 mg/Kg - dry 0.104 0.8093&4 Methylphenol 1 02/03/23 11:15 V29494JMV
<0.176 mg/Kg - dry 0.176 0.809Naphthalene 1 02/03/23 11:15 V29494JMV
<0.118 mg/Kg - dry 0.118 0.8092-Nitroaniline 1 02/03/23 11:15 V29494JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 31
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-032-0031
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 02/01/2023
Holden Brothers Property
Report Date : 02/08/2023
Sample ID :
Lab No :
Sampled:SS-4
98861 Matrix:
1/20/2023 15:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V29430 02/02/23 12:10
<0.146 mg/Kg - dry 0.146 0.8093-Nitroaniline 1 02/03/23 11:15 V29494JMV
<0.114 mg/Kg - dry 0.114 0.4034-Nitroaniline 1 02/03/23 11:15 V29494JMV
<0.141 mg/Kg - dry 0.141 0.403Nitrobenzene 1 02/03/23 11:15 V29494JMV
<0.108 mg/Kg - dry 0.108 0.8092-Nitrophenol 1 02/03/23 11:15 V29494JMV
<0.143 mg/Kg - dry 0.143 0.8094-Nitrophenol 1 02/03/23 11:15 V29494JMV
<0.321 mg/Kg - dry 0.321 0.809N-Nitrosodimethylamine 1 02/03/23 11:15 V29494JMV
<0.221 mg/Kg - dry 0.221 0.809N-Nitrosodiphenylamine 1 02/03/23 11:15 V29494JMV
<0.144 mg/Kg - dry 0.144 0.809N-Nitroso-di-n-propylamine 1 02/03/23 11:15 V29494JMV
<0.424 mg/Kg - dry 0.424 1.22
Pentachlorophenol 1 02/03/23 11:15 V29494JMV
<0.254 mg/Kg - dry 0.254 0.809Phenanthrene 1 02/03/23 11:15 V29494JMV
<0.137 mg/Kg - dry 0.137 0.809Phenol 1 02/03/23 11:15 V29494JMV
<0.164 mg/Kg - dry 0.164 0.809Pyrene 1 02/03/23 11:15 V29494JMV
<0.096 mg/Kg - dry 0.096 0.403Pyridine 1 02/03/23 11:15 V29494JMV
<0.130 mg/Kg - dry 0.130 0.8091,2,4-Trichlorobenzene 1 02/03/23 11:15 V29494JMV
<0.117 mg/Kg - dry 0.117 0.8092,4,5-Trichlorophenol 1 02/03/23 11:15 V29494JMV
<0.118 mg/Kg - dry 0.118 0.809
2,4,6-Trichlorophenol 1 02/03/23 11:15 V29494JMV
8270ESurrogate: Phenol-d5 75.7 Limits: 34-121%02/03/23 11:151 JMV
Surrogate: 2-Fluorobiphenyl 92.2 Limits: 44-115%02/03/23 11:151 JMV V29494
Surrogate: 2-Fluorophenol 83.5 Limits: 35-115%02/03/23 11:151 JMV V29494
Surrogate: Nitrobenzene-d5 107 Limits: 37-122%02/03/23 11:151 JMV V29494
Surrogate: 4-Terphenyl-d14 104 Limits: 54-127%02/03/23 11:151 JMV V29494
Surrogate: 2,4,6-Tribromophenol 97.9 Limits: 39-132%02/03/23 11:151 JMV V29494
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 31
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
23-032-0031
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-2301 Received : 02/01/2023
Holden Brothers Property
Report Date : 02/08/2023
Sample ID :
Lab No :
Sampled:SS-4
98861 Matrix:
1/20/2023 15:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V29431 02/02/23 12:00
<11.3 mg/Kg - dry 11.3 61.2Aliphatic C9-C18 1 02/07/23 12:34 V29557AMP
<14.9 mg/Kg - dry 14.9 61.2Aliphatic C19-C36 1 02/07/23 12:34 V29557AMP
<17.4 mg/Kg - dry 17.4 61.2Aromatic C11-C22 1 02/07/23 12:34 V29557AMP
MADEP-EPHSurrogate: 2-Bromonaphthalene 97.3 Limits: 40-140%02/07/23 12:341 AMP
MADEP-EPHSurrogate: Chlorooctadecane 95.0 Limits: 40-140%02/07/23 12:341 AMP
MADEP-EPHSurrogate: OTP Surrogate 78.5 Limits: 40-140%02/07/23 12:341 AMP
Surrogate: 2-Fluorobiphenyl 100 Limits: 40-140%02/07/23 12:341 AMP V29557
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V29400 02/01/23 08:00
<1.49 mg/Kg - dry 1.49 9.79
Aliphatic C5-C8 100 02/02/23 08:28 V29401TBL
<5.58 mg/Kg - dry 5.58 9.79Aliphatic C9-C12 100 02/02/23 08:28 V29401TBL
<0.763 mg/Kg - dry 0.763 9.79Aromatic C9-C10 100 02/02/23 08:28 V29401TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)80.7 Limits: 70-130%02/02/23 08:28100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)75.0 Limits: 70-130%02/02/23 08:28100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 31
Quality Control Data
23-032-0031Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V29482QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V29481
Associated Lab Samples: 98861
LRB-V29481 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/03/23 10:440.0200.002<0.002mg/KgAcetone
02/03/23 10:440.0200.0008<0.0008mg/KgAcrylonitrile
02/03/23 10:440.0050.0006<0.0006mg/KgBenzene
02/03/23 10:440.0050.0005<0.0005mg/KgBromobenzene
02/03/23 10:440.0050.0008<0.0008mg/KgBromochloromethane
02/03/23 10:440.0050.001<0.001mg/KgBromodichloromethane
02/03/23 10:440.0050.001<0.001mg/KgBromoform
02/03/23 10:440.0100.001<0.001mg/KgBromomethane
02/03/23 10:440.0050.0005<0.0005mg/Kgn-Butylbenzene
02/03/23 10:440.0050.0006<0.0006mg/Kgsec-Butyl benzene
02/03/23 10:440.0050.0005<0.0005mg/Kgtert-Butyl benzene
02/03/23 10:440.0050.0006<0.0006mg/KgCarbon Disulfide
02/03/23 10:440.0050.001<0.001mg/KgCarbon Tetrachloride
02/03/23 10:440.0050.0007<0.0007mg/KgChlorobenzene
02/03/23 10:440.0050.0009<0.0009mg/KgChlorodibromomethane
02/03/23 10:440.0100.0009<0.0009mg/KgChloroethane
02/03/23 10:440.0050.001<0.001mg/KgChloroform
02/03/23 10:440.0100.0006<0.0006mg/KgChloromethane
02/03/23 10:440.0050.0005<0.0005mg/Kg2-Chlorotoluene
02/03/23 10:440.0050.0004<0.0004mg/Kg4-Chlorotoluene
02/03/23 10:440.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
02/03/23 10:440.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
02/03/23 10:440.0050.0006<0.0006mg/Kg1,2-Dibromoethane
02/03/23 10:440.0050.0006<0.0006mg/KgDibromomethane
02/03/23 10:440.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
02/03/23 10:440.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
02/03/23 10:440.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
Page 1 of 15Date:02/08/2023 04:10 PM
Page 15 of 31
Quality Control Data
23-032-0031Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V29482QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V29481
Associated Lab Samples: 98861
LRB-V29481 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/03/23 10:440.0100.001<0.001mg/KgDichlorodifluoromethane
02/03/23 10:440.0050.0008<0.0008mg/Kg1,1-Dichloroethane
02/03/23 10:440.0050.001<0.001mg/Kg1,2-Dichloroethane
02/03/23 10:440.0050.0007<0.0007mg/Kg1,1-Dichloroethene
02/03/23 10:440.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
02/03/23 10:440.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
02/03/23 10:440.0050.0004<0.0004mg/Kg1,2-Dichloropropane
02/03/23 10:440.0050.0006<0.0006mg/Kg1,3-Dichloropropane
02/03/23 10:440.0050.001<0.001mg/Kg2,2-Dichloropropane
02/03/23 10:440.0050.0008<0.0008mg/Kg1,1-Dichloropropene
02/03/23 10:440.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
02/03/23 10:440.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
02/03/23 10:440.0050.0006<0.0006mg/KgEthylbenzene
02/03/23 10:440.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
02/03/23 10:440.0100.0008<0.0008mg/KgHexachlorobutadiene
02/03/23 10:440.0100.0007<0.0007mg/Kgn-Hexane
02/03/23 10:440.0200.0006<0.0006mg/Kg2-Hexanone
02/03/23 10:440.0050.0005<0.0005mg/KgIsopropylbenzene
02/03/23 10:440.0050.001<0.001mg/Kg4-Isopropyl toluene
02/03/23 10:440.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
02/03/23 10:440.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
02/03/23 10:440.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
02/03/23 10:440.0100.001<0.001mg/KgMethylene Chloride
02/03/23 10:440.0100.0010<0.0010mg/KgNaphthalene
02/03/23 10:440.0050.0005<0.0005mg/Kgn-Propylbenzene
02/03/23 10:440.0050.001<0.001mg/KgStyrene
02/03/23 10:440.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
Page 2 of 15Date:02/08/2023 04:10 PM
Page 16 of 31
Quality Control Data
23-032-0031Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V29482QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V29481
Associated Lab Samples: 98861
LRB-V29481 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/03/23 10:440.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
02/03/23 10:440.0050.0009<0.0009mg/KgTetrachloroethene
02/03/23 10:440.0050.0007<0.0007mg/KgToluene
02/03/23 10:440.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
02/03/23 10:440.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
02/03/23 10:440.0050.001<0.001mg/Kg1,1,1-Trichloroethane
02/03/23 10:440.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
02/03/23 10:440.0050.0009<0.0009mg/KgTrichloroethene
02/03/23 10:440.0100.002<0.002mg/KgTrichlorofluoromethane
02/03/23 10:440.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
02/03/23 10:440.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
02/03/23 10:440.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
02/03/23 10:440.0100.0005<0.0005mg/KgVinyl Acetate
02/03/23 10:440.0100.0005<0.0005mg/KgVinyl Chloride
02/03/23 10:440.0050.0005<0.0005mg/Kgo-Xylene
02/03/23 10:440.0100.001<0.001mg/Kgm,p-Xylene
02/03/23 10:444-Bromofluorobenzene (S)104 70-130
02/03/23 10:44Dibromofluoromethane (S)104 84-123
02/03/23 10:44Toluene-d8 (S)95.6 76-129
LCS-V29481Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
71.70.0710.100mg/KgAcrolein 70-130
Page 3 of 15Date:02/08/2023 04:10 PM
Page 17 of 31
Quality Control Data
23-032-0031Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V29482QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V29481
LCS-V29481 LCSD-V29481Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.094 94.998.80.0980.100mg/KgAcetone 29-198 4.0 20
0.104 10497.10.0970.100mg/KgAcrylonitrile 65-134 6.8 20
0.049 98.01050.0520.050mg/KgBenzene 74-127 6.7 20
0.046 93.694.60.0470.050mg/KgBromobenzene 73-125 1.0 20
0.052 1061100.0550.050mg/KgBromochloromethane 72-134 4.0 20
0.049 99.81030.0510.050mg/KgBromodichloromethane 75-122 3.1 20
0.051 1031020.0510.050mg/KgBromoform 66-135 0.3 20
0.049 98.287.60.0430.050mg/KgBromomethane 20-180 11.4 20
0.046 93.298.20.0490.050mg/Kgn-Butylbenzene 65-135 5.2 20
0.044 88.293.60.0460.050mg/Kgsec-Butyl benzene 66-131 5.9 20
0.043 87.693.80.0460.050mg/Kgtert-Butyl benzene 67-132 6.8 20
0.046 93.698.20.0490.050mg/KgCarbon Disulfide 61-129 4.7 20
0.050 1011080.0540.050mg/KgCarbon Tetrachloride 64-143 7.0 20
0.048 96.01010.0500.050mg/KgChlorobenzene 74-118 4.8 20
0.050 1011040.0520.050mg/KgChlorodibromomethane 73-122 3.3 20
0.041 82.884.60.0420.050mg/KgChloroethane 33-149 2.1 20
0.047 95.61000.0500.050mg/KgChloroform 73-127 4.4 20
0.043 86.098.40.0490.050mg/KgChloromethane 45-143 13.4 20
0.044 89.694.00.0470.050mg/Kg2-Chlorotoluene 67-124 4.7 20
0.044 89.694.00.0470.050mg/Kg4-Chlorotoluene 71-126 4.7 20
0.048 96.898.80.0490.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.0 20
0.047 95.695.00.0470.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 0.6 20
0.049 99.097.40.0480.050mg/Kg1,2-Dibromoethane 70-132 1.6 20
0.051 1031040.0510.050mg/KgDibromomethane 74-133 0.7 20
0.047 95.297.00.0480.050mg/Kg1,2-Dichlorobenzene 72-123 1.8 20
0.046 92.493.60.0460.050mg/Kg1,3-Dichlorobenzene 71-120 1.2 20
Page 4 of 15Date:02/08/2023 04:10 PM
Page 18 of 31
Quality Control Data
23-032-0031Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V29482QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V29481
LCS-V29481 LCSD-V29481Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 89.894.20.0470.050mg/Kg1,4-Dichlorobenzene 71-123 4.7 20
0.047 94.61030.0510.050mg/KgDichlorodifluoromethane 26-146 8.8 20
0.048 97.41010.0500.050mg/Kg1,1-Dichloroethane 74-127 4.0 20
0.051 1031000.0500.050mg/Kg1,2-Dichloroethane 68-128 2.5 20
0.045 90.897.60.0480.050mg/Kg1,1-Dichloroethene 67-149 7.2 20
0.051 1021010.0500.050mg/Kgcis-1,2-Dichloroethene 76-134 0.9 20
0.049 99.81010.0500.050mg/Kgtrans-1,2-Dichloroethene 73-132 1.3 20
0.049 99.299.40.0490.050mg/Kg1,2-Dichloropropane 73-130 0.2 20
0.050 1011020.0500.050mg/Kg1,3-Dichloropropane 75-124 0.7 20
0.046 93.21010.0500.050mg/Kg2,2-Dichloropropane 50-142 7.8 20
0.049 98.01030.0510.050mg/Kg1,1-Dichloropropene 71-130 4.7 20
0.052 1041060.0530.050mg/Kgcis-1,3-Dichloropropene 71-125 1.9 20
0.054 1091080.0530.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.7 20
0.047 94.696.80.0480.050mg/KgEthylbenzene 74-128 2.2 20
0.099 99.41010.1010.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 1.5 20
0.044 89.693.40.0460.050mg/KgHexachlorobutadiene 64-125 4.1 20
0.048 97.01010.0500.050mg/Kgn-Hexane 70-130 4.2 20
0.044 88.892.00.0460.050mg/Kg2-Hexanone 61-157 3.5 20
0.044 88.894.40.0470.050mg/KgIsopropylbenzene 68-126 6.1 20
0.045 90.496.20.0480.050mg/Kg4-Isopropyl toluene 68-129 6.2 20
0.048 97.094.80.0470.050mg/KgMethyl Ethyl Ketone (MEK)63-149 2.2 20
0.049 98.21010.0500.050mg/KgMethyl tert-butyl ether (MTBE)70-130 2.4 20
0.051 1031030.0510.050mg/Kg4-Methyl-2-Pentanone 57-162 0.1 20
0.046 92.093.20.0460.050mg/KgMethylene Chloride 74-129 1.2 20
0.045 90.092.00.0460.050mg/KgNaphthalene 57-157 2.1 20
0.044 89.895.40.0470.050mg/Kgn-Propylbenzene 67-130 6.0 20
Page 5 of 15Date:02/08/2023 04:10 PM
Page 19 of 31
Quality Control Data
23-032-0031Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V29482QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V29481
LCS-V29481 LCSD-V29481Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.050 1011020.0500.050mg/KgStyrene 77-121 0.5 20
0.049 99.299.80.0490.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.6 20
0.044 89.688.80.0440.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 0.8 20
0.047 94.898.60.0490.050mg/KgTetrachloroethene 68-130 3.9 20
0.049 99.01030.0510.050mg/KgToluene 71-129 3.5 20
0.044 89.287.40.0430.050mg/Kg1,2,3-Trichlorobenzene 68-130 2.0 20
0.048 97.895.20.0470.050mg/Kg1,2,4-Trichlorobenzene 66-125 2.6 20
0.047 94.41020.0500.050mg/Kg1,1,1-Trichloroethane 67-131 7.3 20
0.049 98.21040.0520.050mg/Kg1,1,2-Trichloroethane 70-133 6.1 20
0.045 91.81020.0510.050mg/KgTrichloroethene 75-133 10.5 20
0.042 84.891.40.0450.050mg/KgTrichlorofluoromethane 44-146 7.4 20
0.047 95.894.60.0470.050mg/Kg1,2,3-Trichloropropane 60-137 1.2 20
0.046 92.695.60.0470.050mg/Kg1,2,4-Trimethylbenzene 69-129 3.1 20
0.044 89.094.80.0470.050mg/Kg1,3,5-Trimethylbenzene 69-128 6.3 20
0.035 71.063.00.0310.050mg/KgVinyl Acetate 60-140 11.9 20
0.037 74.881.40.0400.050mg/KgVinyl Chloride 48-147 8.4 20
0.048 96.097.20.0480.050mg/Kgo-Xylene 74-126 1.2 20
0.095 95.298.40.0980.100mg/Kgm,p-Xylene 75-124 3.3 20
1031024-Bromofluorobenzene (S)70-130
102101Dibromofluoromethane (S)84-123
10098.0Toluene-d8 (S)76-129
Page 6 of 15Date:02/08/2023 04:10 PM
Page 20 of 31
Quality Control Data
23-032-0031Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V29494QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29430
Associated Lab Samples: 98861
LRB-V29430 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/03/23 09:200.6600.116<0.116mg/KgAcenaphthene
02/03/23 09:200.6600.105<0.105mg/KgAcenaphthylene
02/03/23 09:200.6600.152<0.152mg/KgAniline
02/03/23 09:200.6600.143<0.143mg/KgAnthracene
02/03/23 09:200.6600.139<0.139mg/KgBenzo(a)anthracene
02/03/23 09:200.6600.147<0.147mg/KgBenzo(a)pyrene
02/03/23 09:200.6600.146<0.146mg/KgBenzo(b)fluoranthene
02/03/23 09:200.6600.136<0.136mg/KgBenzo(g,h,i)perylene
02/03/23 09:200.6600.137<0.137mg/KgBenzo(k)fluoranthene
02/03/23 09:202.000.580<0.580mg/KgBenzoic Acid
02/03/23 09:200.6600.105<0.105mg/KgBenzyl alcohol
02/03/23 09:200.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
02/03/23 09:200.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
02/03/23 09:200.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
02/03/23 09:200.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
02/03/23 09:200.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
02/03/23 09:200.3300.113<0.113mg/KgButyl benzyl phthalate
02/03/23 09:200.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
02/03/23 09:200.3300.112<0.112mg/Kg4-Chloroaniline
02/03/23 09:200.6600.116<0.116mg/Kg2-Chloronaphthalene
02/03/23 09:200.6600.098<0.098mg/Kg2-Chlorophenol
02/03/23 09:201.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
02/03/23 09:200.6600.142<0.142mg/KgChrysene
02/03/23 09:200.6600.230<0.230mg/KgDibenz(a,h)anthracene
02/03/23 09:200.6600.119<0.119mg/KgDibenzofuran
02/03/23 09:200.6600.094<0.094mg/Kg1,2-Dichlorobenzene
02/03/23 09:200.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 7 of 15Date:02/08/2023 04:10 PM
Page 21 of 31
Quality Control Data
23-032-0031Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V29494QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29430
Associated Lab Samples: 98861
LRB-V29430 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/03/23 09:200.3300.097<0.097mg/Kg1,4-Dichlorobenzene
02/03/23 09:200.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
02/03/23 09:200.6600.095<0.095mg/Kg2,4-Dichlorophenol
02/03/23 09:200.6600.180<0.180mg/KgDiethyl phthalate
02/03/23 09:200.6600.174<0.174mg/KgDimethyl phthalate
02/03/23 09:200.3300.108<0.108mg/Kg2,4-Dimethylphenol
02/03/23 09:200.6600.107<0.107mg/KgDi-n-butyl phthalate
02/03/23 09:201.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
02/03/23 09:201.500.520<0.520mg/Kg2,4-Dinitrophenol
02/03/23 09:200.6600.096<0.096mg/Kg2,4-Dinitrotoluene
02/03/23 09:200.6600.108<0.108mg/Kg2,6-Dinitrotoluene
02/03/23 09:200.3300.143<0.143mg/KgDi-n-Octyl Phthalate
02/03/23 09:200.6600.123<0.123mg/KgFluoranthene
02/03/23 09:200.6600.128<0.128mg/KgFluorene
02/03/23 09:200.6600.106<0.106mg/KgHexachlorobenzene
02/03/23 09:200.6600.097<0.097mg/KgHexachlorobutadiene
02/03/23 09:200.6600.157<0.157mg/KgHexachlorocyclopentadiene
02/03/23 09:200.6600.079<0.079mg/KgHexachloroethane
02/03/23 09:200.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
02/03/23 09:200.6600.191<0.191mg/KgIsophorone
02/03/23 09:200.6600.106<0.106mg/Kg1-Methylnaphthalene
02/03/23 09:200.6600.100<0.100mg/Kg2-Methylnaphthalene
02/03/23 09:200.6600.097<0.097mg/Kg2-Methylphenol
02/03/23 09:200.6600.084<0.084mg/Kg3&4 Methylphenol
02/03/23 09:200.6600.144<0.144mg/KgNaphthalene
02/03/23 09:200.6600.096<0.096mg/Kg2-Nitroaniline
02/03/23 09:200.6600.120<0.120mg/Kg3-Nitroaniline
Page 8 of 15Date:02/08/2023 04:10 PM
Page 22 of 31
Quality Control Data
23-032-0031Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V29494QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29430
Associated Lab Samples: 98861
LRB-V29430 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/03/23 09:200.3300.093<0.093mg/Kg4-Nitroaniline
02/03/23 09:200.3300.116<0.116mg/KgNitrobenzene
02/03/23 09:200.6600.088<0.088mg/Kg2-Nitrophenol
02/03/23 09:200.6600.117<0.117mg/Kg4-Nitrophenol
02/03/23 09:200.6600.263<0.263mg/KgN-Nitrosodimethylamine
02/03/23 09:200.6600.181<0.181mg/KgN-Nitrosodiphenylamine
02/03/23 09:200.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
02/03/23 09:201.000.347<0.347mg/KgPentachlorophenol
02/03/23 09:200.6600.208<0.208mg/KgPhenanthrene
02/03/23 09:200.6600.112<0.112mg/KgPhenol
02/03/23 09:200.6600.134<0.134mg/KgPyrene
02/03/23 09:200.3300.079<0.079mg/KgPyridine
02/03/23 09:200.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
02/03/23 09:200.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
02/03/23 09:200.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
02/03/23 09:202-Fluorobiphenyl (S)92.8 44-115
02/03/23 09:202-Fluorophenol (S)84.3 35-115
02/03/23 09:20Nitrobenzene-d5 (S)104 37-122
02/03/23 09:204-Terphenyl-d14 (S)111 54-127
02/03/23 09:202,4,6-Tribromophenol (S)93.6 39-132
02/03/23 09:20Phenol-d5 (S)76.2 34-121
LCS-V29430 LCSD-V29430Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.52 91.093.41.561.67mg/KgAcenaphthene 40-123 2.5 20
Page 9 of 15Date:02/08/2023 04:10 PM
Page 23 of 31
Quality Control Data
23-032-0031Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V29494QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29430
LCS-V29430 LCSD-V29430Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.60 95.898.21.641.67mg/KgAcenaphthylene 32-132 2.4 20
2.31 1381432.391.67mg/KgAniline 12-197 3.4 20
1.65 98.81011.681.67mg/KgAnthracene 47-123 1.8 20
1.68 1011011.691.67mg/KgBenzo(a)anthracene 49-126 0.5 20
1.81 1081111.861.67mg/KgBenzo(a)pyrene 45-129 2.7 20
1.75 1051081.811.67mg/KgBenzo(b)fluoranthene 45-132 3.3 20
1.58 94.696.41.611.67mg/KgBenzo(g,h,i)perylene 43-134 1.8 20
1.66 99.41031.721.67mg/KgBenzo(k)fluoranthene 47-132 3.5 20
1.60 95.8*97.6*1.631.67mg/KgBenzoic Acid 10-83 1.8 20
1.53 91.693.41.561.67mg/KgBenzyl alcohol 29-122 1.9 20
1.56 93.492.81.551.67mg/KgBis(2-Chloroethoxy)methane 36-121 0.6 20
1.42 85.086.21.441.67mg/KgBis(2-Chloroethyl)ether 31-120 1.3 20
1.45 86.889.21.491.67mg/KgBis(2-Chloroisopropyl)ether 33-131 2.7 20
1.95 1171191.991.67mg/KgBis(2-ethylhexyl)phthalate 51-133 2.0 20
1.61 96.41011.681.67mg/Kg4-Bromophenyl phenyl ether 46-124 4.2 20
1.85 1111151.921.67mg/KgButyl benzyl phthalate 48-132 3.7 20
1.65 98.81011.691.67mg/Kg4-Chloro-3-methylphenol 45-122 2.3 20
1.40 83.888.61.481.67mg/Kg4-Chloroaniline 17-106 5.5 20
1.56 93.495.21.591.67mg/Kg2-Chloronaphthalene 41-114 1.9 20
1.53 91.692.81.551.67mg/Kg2-Chlorophenol 34-121 1.2 20
1.61 96.498.81.651.67mg/Kg4-Chlorophenyl phenyl ether 45-121 2.4 20
1.50 89.891.61.531.67mg/KgChrysene 50-124 1.9 20
1.72 1031081.801.67mg/KgDibenz(a,h)anthracene 45-134 4.5 20
1.56 93.496.41.611.67mg/KgDibenzofuran 44-120 3.1 20
1.36 81.483.81.401.67mg/Kg1,2-Dichlorobenzene 33-117 2.8 20
1.35 80.880.21.341.67mg/Kg1,3-Dichlorobenzene 30-115 0.7 20
Page 10 of 15* QC Fail Date:02/08/2023 04:10 PM
Page 24 of 31
Quality Control Data
23-032-0031Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V29494QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29430
LCS-V29430 LCSD-V29430Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.35 80.882.61.381.67mg/Kg1,4-Dichlorobenzene 31-115 2.1 20
1.47 88.091.61.531.67mg/Kg3,3'-Dichlorobenzidine 22-121 4.0 20
1.63 97.699.41.661.67mg/Kg2,4-Dichlorophenol 40-122 1.8 20
1.67 1001021.711.67mg/KgDiethyl phthalate 50-124 2.3 20
1.64 98.21031.721.67mg/KgDimethyl phthalate 48-124 4.7 20
1.98 1191262.101.67mg/Kg2,4-Dimethylphenol 30-127 5.8 20
1.87 1121161.931.67mg/KgDi-n-butyl phthalate 51-128 3.1 20
2.03 1221232.051.67mg/Kg4,6-Dinitro-2-methylphenol 29-132 0.9 20
1.81 1081101.831.67mg/Kg2,4-Dinitrophenol 27-129 1.0 20
1.95 1171222.041.67mg/Kg2,4-Dinitrotoluene 48-126 4.5 20
1.76 1051061.771.67mg/Kg2,6-Dinitrotoluene 46-124 0.5 20
2.09 1251312.191.67mg/KgDi-n-Octyl Phthalate 45-140 4.6 20
1.55 92.895.21.591.67mg/KgFluoranthene 50-127 2.5 20
1.62 97.097.61.631.67mg/KgFluorene 43-125 0.6 20
1.58 94.695.81.601.67mg/KgHexachlorobenzene 45-122 1.2 20
1.51 90.492.81.551.67mg/KgHexachlorobutadiene 32-123 2.6 20
1.24 74.276.61.281.67mg/KgHexachlorocyclopentadiene 32-117 3.1 20
1.33 79.681.41.361.67mg/KgHexachloroethane 28-117 2.2 20
1.70 1021041.741.67mg/KgIndeno(1,2,3-cd)pyrene 45-133 2.3 20
0.956 57.258.60.9791.67mg/KgIsophorone 30-122 2.3 20
1.47 88.088.61.481.67mg/Kg1-Methylnaphthalene 40-119 0.6 20
1.46 87.488.61.481.67mg/Kg2-Methylnaphthalene 38-122 1.3 20
1.54 92.293.41.561.67mg/Kg2-Methylphenol 32-122 1.2 20
1.43 85.686.81.451.67mg/Kg3&4 Methylphenol 34-119 1.3 20
1.45 86.886.21.441.67mg/KgNaphthalene 35-123 0.6 20
1.86 1111181.971.67mg/Kg2-Nitroaniline 44-127 5.7 20
Page 11 of 15Date:02/08/2023 04:10 PM
Page 25 of 31
Quality Control Data
23-032-0031Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V29494QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29430
LCS-V29430 LCSD-V29430Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.86 1111181.971.67mg/Kg3-Nitroaniline 33-119 5.7 20
1.82 1091131.881.67mg/Kg4-Nitroaniline 63-147 3.2 20
1.64 98.297.61.631.67mg/KgNitrobenzene 34-122 0.6 20
1.98 1191202.011.67mg/Kg2-Nitrophenol 36-123 1.5 20
1.66 99.41041.731.67mg/Kg4-Nitrophenol 30-132 4.1 20
1.22 73.076.01.271.67mg/KgN-Nitrosodimethylamine 10-146 4.0 20
1.95 1171202.011.67mg/KgN-Nitrosodiphenylamine 38-127 3.0 20
1.45 86.889.21.491.67mg/KgN-Nitroso-di-n-propylamine 36-120 2.7 20
1.90 1141171.951.67mg/KgPentachlorophenol 25-133 2.5 20
1.62 97.01001.671.67mg/KgPhenanthrene 50-121 3.0 20
1.51 90.490.41.511.67mg/KgPhenol 34-121 0.0 20
1.63 97.61011.691.67mg/KgPyrene 47-127 3.6 20
1.05 62.862.81.051.67mg/KgPyridine 10-80 0.0 20
1.40 83.886.21.441.67mg/Kg1,2,4-Trichlorobenzene 34-118 2.8 20
1.75 1051081.801.67mg/Kg2,4,5-Trichlorophenol 41-124 2.8 20
1.65 98.81011.691.67mg/Kg2,4,6-Trichlorophenol 39-126 2.3 20
93.496.42-Fluorobiphenyl (S)44-115
81.682.52-Fluorophenol (S)35-115
103102Nitrobenzene-d5 (S)37-122
1011034-Terphenyl-d14 (S)54-127
96.01012,4,6-Tribromophenol (S)39-132
74.776.8Phenol-d5 (S)34-121
Page 12 of 15Date:02/08/2023 04:10 PM
Page 26 of 31
Quality Control Data
23-032-0031Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V29557QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V29431
Associated Lab Samples: 98861
LRB-V29431 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/07/23 10:4550.09.20<9.20mg/KgAliphatic C9-C18
02/07/23 10:4550.012.2<12.2mg/KgAliphatic C19-C36
02/07/23 10:4550.014.2<14.2mg/KgAromatic C11-C22
02/07/23 10:452-Fluorobiphenyl (S)94.7 40-140
02/07/23 10:452-Bromonaphthalene (S)92.7 40-140
02/07/23 10:45Chlorooctadecane (S)90.5 40-140
02/07/23 10:45OTP Surrogate (S)81.0 40-140
LCS-V29431 LCSD-V29431Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
49.2 82.076.545.960.0mg/KgAliphatic C9-C18 40-140 6.9 50
82.7 10396.377.180.0mg/KgAliphatic C19-C36 40-140 7.0 50
192 11398.8168170mg/KgAromatic C11-C22 40-140 13.3 50
1081062-Fluorobiphenyl (S)40-140
1081062-Bromonaphthalene (S)40-140
113102Chlorooctadecane (S)40-140
91.086.5OTP Surrogate (S)40-140
Page 13 of 15Date:02/08/2023 04:10 PM
Page 27 of 31
Quality Control Data
23-032-0031Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V29401QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V29400
Associated Lab Samples: 98861
LRB-V29400 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/01/23 17:068.001.22<1.22mg/KgAliphatic C5-C8
02/01/23 17:068.004.56<4.56mg/KgAliphatic C9-C12
02/01/23 17:068.000.624<0.624mg/KgAromatic C9-C10
02/01/23 17:062,5-Dibromotoluene (FID) (S)92.7 70-130
02/01/23 17:062,5-Dibromotoluene (PID) (S)89.2 70-130
LCS-V29400 LCSD-V29400Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
31.3 97.896.831.032.0mg/KgAliphatic C5-C8 70-130 0.9 50
37.6 11811938.132.0mg/KgAliphatic C9-C12 70-130 1.3 50
12.0 11211212.010.7mg/KgAromatic C9-C10 70-130 0.0 50
84.980.22,5-Dibromotoluene (FID) (S)70-130
79.777.52,5-Dibromotoluene (PID) (S)70-130
Page 14 of 15Date:02/08/2023 04:10 PM
Page 28 of 31
Quality Control Data
23-032-0031Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Holden Brothers Property
Dry Weight Determination
SW-DRYWT
V29409QC Analytical Batch:
Analysis Method:
Analysis Description:
V 98861-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 02/02/23 11:301.618.018.3%Moisture
V 98863-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 02/02/23 11:301.532.633.1%Moisture
Page 15 of 15Date:02/08/2023 04:10 PM
Page 29 of 31
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-032-0031
Paragon Environmental Consultants, Inc.
01156
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 2.7C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:02/01/2023 17:05:08
Special precautions or instructions included?
Comments:
Page 30 of 31
Page 31 of 31

APPENDIX C

STANDARD OPERATING PROCEDURES

STANDARD OPERATING PROCEDURES
PARAGON ENVIRONMENTAL CONSULTANTS, INC.

I. SOIL SAMPLE PROCEDURES
1. Collect all samples using disposable Latex gloves. Gloves are not to be re- used. 2. Place samples into laboratory supplied glassware following requirements for specific analysis. 3. Label samples with sample ID, date, time, and job number. Immediately place samples on ice or in refrigerator to be cooled to approximately 4 degrees Celsius. 4. Store all samples on ice or refrigerate until samples are delivered to the laboratory. 5. Complete a chain of custody record for samples to be submitted to laboratory. Sign and date the chain of custody when samples are relinquished in accordance with EPA chain of custody protocol. II. GROUNDWATER SAMPLING 1. Use new disposable bailer and new nylon string to develop well and collect sample. Handle bailer and string with Latex gloves. 2. Develop well by removing 3 well volumes of water. Dispose of water in accordance with NCDEQ guidelines. 3. Following well development obtain samples in laboratory supplied glassware following requirements for specific analysis. 4. Handle, store, and transport samples in same manner as for soil samples. See items I.3, I.4, and I.5 above. III. EQUIPMENT CONTAMINATION 1. Decontaminate augers, split spoons, and other sampling equipment by the following procedure: A. Soap and tap water wash B. Tap water rinse C. Distilled deionized water rinse D. Isopropyl alcohol rinse E. Distilled water rinse 2. Use new disposable sampling equipment whenever practical.
SOP

APPENDIX D

SOIL DISPOSAL MANIFESTS