WS-96235_96816_CA_IAR_20230127

Initial Abatement Action Report
Yadkin County Solid Waste
Transfer Facility
Yadkinville, North Carolina
S&ME Project No. 22580534
PREPARED FOR:
Yadkin County
217 E. Willow Street
Yadkinville, North Carolina 27055
PREPARED BY:
S&ME, Inc.
8646 West Market Street, Suite 105
Greensboro, North Carolina 27409
January 27, 2022

Initial Abatement Action Report
Yadkin County Solid Waste Transfer Facility
Yadkinville, North Carolina
S&ME Project No. 22580534
January 27, 2023 iii
1.0 Site Information
1.1 Site Identification
Date of Report: 1/27/2023 Site Risk: Pending
Facility I.D.: N/A AST Incident Number: 96816
Site Name: Yadkin County Solid Waste Transfer Station
Street Address: 1149 Landfill Road, Yadkinville, North Carolina
City/Town: Yadkinville Zip Code: 27055 County: Yadkin
Description of Geographical Data Point (e.g., diesel fill port): AST
Location Method (GPS, topographical map, other): Google Earth
Latitude (degrees): 36.181267 Longitude (degrees): -80.6415
1.2 Information about Contacts Associated with the Leaking UST System
UST/AST Owner: Yadkin County Email: N/A
Address: 1149 Landfill Road Yadkinville, NC 27055 Tel: [phone]
Property Owner: Yadkin County Email: N/A
Address: 1149 Landfill Road Yadkinville, NC 27055 Tel: [phone]
Property Occupant: Yadkin County Email: N/A
Address: 1149 Landfill Road Yadkinville, NC 27055 Tel: [phone]
Consultant/Contractor: Wayne Watterson Email: [e-mail]
Address: 8646 W. Market Street Ste. 105, Greensboro, NC 27409 Tel: [phone]
Analytical Laboratory: Eurofins Savannah State Certification No: 314
Address: 5102 LaRoche Avenue, Savannah, GA 311404 Tel: [phone]
1.3 Information about the Release
Date Discovered: 8/26/2022
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release (e.g., Dispenser/Piping/UST): Unknown
Size and Contents of Tank: Used Oil AST

Excavation and Sample Date: 12/05/2022

Initial Abatement Action Report
Yadkin County Solid Waste Transfer Facility
Yadkinville, North Carolina
S&ME Project No. 22580534
January 27, 2023 iv

Table of Contents
1.0 Site Information .............................................................................................................. iii
1.1 Site Identification .......................................................................................................................... iii
1.2 Information about Contacts Associated with the Leaking UST System ............................... iii
1.3 Information about the Release .................................................................................................... iii
2.0 Scope of Services ............................................................................................................... 1
3.0 Site History and Characterization ................................................................................. 1
Table 1.1. AST Owner ................................................................................................................................................. 1
4.0 Free Product Investigation and Recovery Report ....................................................... 1
5.0 Initial Response and Abatement Action ...................................................................... 2
5.1 Soil Excavation ................................................................................................................................ 2
5.2 Soil Sampling and Laboratory Analysis ...................................................................................... 2
6.0 Conclusions and Recommendations ............................................................................. 3

List of Figures
Figure 1- USGS Topographic Map
Figure 2- Site Map
Figure 3- Soil Sample Locations

List of Tables
Table 1- Summary of Soil Sampling Results

Appendices
Appendix I –Figures
Appendix II –Tables
Appendix III - Notice of Regulatory Requirements (September 22, 2022)
Appendix IV - Non-Hazardous Materials Manifests
Appendix V - Analytical Laboratory Report
Initial Abatement Action Report
Yadkin County Solid Waste Transfer Facility
Yadkinville, North Carolina
S&ME Project No. 22580534
January 27, 2022 1
2.0 Scope of Services
The Scope of Services for this project included S&ME’s collection of one characterization soil sample, observance
of the excavation of petroleum-impacted soils by subcontractor Buckeye-Elm Contracting, LLC, and collection of
one confirmation soil sample from below the base of the excavation conducted to remove surface-stained soils.
3.0 Site History and Characterization
The subject site is located at 1149 Landfill Road, Yadkinville, North Carolina as depicted on Figure 1 included in
Appendix I. A Site Map (Figure 2) and a Soil Sample Locations Map (Figure 3) are included in Appendix I.
The Yadkin County Solid Waste Transfer Facility serves as an acceptance facility for bagged trash, recyclables,
construction and demolition debris, yard waste, metal, tires, electronics, and motor oil for residents and businesses
of Yadkin County. Based upon the Yadkin County GIS topographic data reviewed, the area in the vicinity of the
AST slopes downward to the east (see Figure 1, Appendix I).
A Facility Compliance Inspection of the Yadkin County Solid Waste Facility (Facility) performed by the North
Carolina Department of Environmental Quality (NCDEQ) on August 26, 2022, identified evidence of oil escaping
from the containment pad of a waste oil above ground storage tank, as indicated by an area of stained soil
approximately 3 feet by 9 feet in dimensions.
A Notice of Regulatory Requirements from the NCDEQ, dated September 20, 2022, was issued in response to the
observation of petroleum staining at the above ground storage tank at the Yadkin County Solid Waste Transfer
Station. The NCDEQ requested an Initial Assessment Report be prepared in accordance with the UST Section
Guidelines for the Investigation and Remediation of Contamination from Non-UST Petroleum Releases.
AST information is provided below in Table 1.1.
Table 1.1. AST Owner
Facility ID No. Name of Owner Street Address Telephone Dates of Operation
9903T-TRANSFER-
1994
Yadkin County 1149 Landfill Road
Yadkinville, NC 27055
336-849-
7912
Unknown-Currently
Operating

4.0 Free Product Investigation and Recovery Report
No free product was encountered during these activities.
Initial Abatement Action Report
Yadkin County Solid Waste Transfer Facility
Yadkinville, North Carolina
S&ME Project No. 22580534
January 27, 2022 2
5.0 Initial Response and Abatement Action
5.1 Soil Excavation
On December 5, 2022, S&ME observed and documented the over excavation of stained soils observed at the
ground surface in the vicinity of the suspect petroleum impacted soil. The excavation activities were conducted by
Buckeye Elm Contracting. During the soil excavation activities, S&ME monitored the excavated soils for evidence
of petroleum impacts by observing for staining and odors. The surface-stained soils excavation was deemed
completed when field observations provided no indications of suspect petroleum impacts remaining in the soil.
Approximately 1-1.5 feet of topsoil was underlain by approximately 0.5-1 feet of coarse gravel underlain by a layer
of woven fabric. Petroleum impacted soil was not observed under the woven fabric barrier at approximately 2-2.5
feet below ground level. Petroleum odors and staining were observed within the gravel that was overlaying the
layer of woven fabric at the limits of the excavation on all sides.. Staining and odors were not observed within the
topsoil overlaying the gravel on all sides of the limits of the excavation.
The surface-stained soil excavation measured approximately 7 feet by 15 feet by 2.5 feet deep. Approximately 10
cubic yards of petroleum-impacted soils were excavated, stockpiled on-site on plastic, and covered with plastic for
temporary storage. The excavation was backfilled with clean soil from on-site, strawed and seeded.
Buckeye-Elm completed a soil profile for disposal, and on January 3, 2023, 14.23 tons of suspect petroleum
impacted soil was transported to EVO Corporation, a permitted disposal facility in Winston Salem, North Carolina.
Copies of the Non-Hazardous Materials manifests are included in Appendix IV.
5.2 Soil Sampling and Laboratory Analysis
S&ME collected one soil sample (SS-C) from the excavated soil on December 5, 2022 for characterization
purposes. The soil sample was collected from the backhoe operated by Buckeye Elm Contracting. The soil sample
was transferred to laboratory-prepared containers by hand using nitrile gloves. The containers were labeled and
stored on ice in a cooler.
S&ME collected one soil sample (SS-B) from directly below the floor of the excavation for laboratory analysis on
December 5, 2022. Soil sample locations are shown on Figure 3. Soil samples were collected with a backhoe
operated by Buckeye Elm Contracting. The soil samples were transferred to laboratory-prepared containers by
hand using nitrile gloves. The containers were labeled and stored on ice in a cooler.
The cooler was delivered to Eurofins analytical laboratory, a North Carolina-certified laboratory, by courier under
chain-of-custody procedures on December 6, 2022.
Soil sample SS-C was analyzed in the laboratory for volatile organic compounds (VOCs) by the 8260 method,
semi-volatile organic compounds (SVOCs) by the 8270 method, and for Resource Recovery and Conservation Act
(RCRA) eight metals by the Toxic Characteristic Leaching Procedure (TCLP) method.
Initial Abatement Action Report
Yadkin County Solid Waste Transfer Facility
Yadkinville, North Carolina
S&ME Project No. 22580534
January 27, 2022 3
Soil sample SS-B was analyzed in the laboratory total petroleum hydrocarbons (TPH) gasoline range organics
(GRO) and TPH diesel range organics (DRO).
Table 1 in Appendix II summarizes the results of laboratory analyses performed on the soil samples collected
from the soil excavation. A copy of the laboratory analytical report and chain-of-custody is included in Appendix
V. Analytical results for the soil sample collected from the petroleum impacted soil indicate no target analytes
were reported at concentrations greater than North Carolina Department of Environmental Quality (NCDEQ) soil-
to-water Maximum Soil Contaminant Concentrations (MSCCs). Analytical results for the soil sample collected at
the base of the excavation were reported at concentrations less than the NCDEQ TPH-GRO and TPH-DRO actions
levels of 50 mg/kg and 100 mg/kg respectively.
6.0 Conclusions and Recommendations
On December 5, 2022, S&ME observed the excavation of the surface-stained soils east of the used oil AST. The
surface-stained soil excavation measured approximately 7 feet by 15 feet by 2.5 feet deep.
Analytical results for the soil samples obtained at the base of the surface-stained soil excavation indicated TPH-
GRO and TPH-DRO concentrations are less than the NCDEQ action limits of 50 mg/kg and 100 mg/kg
respectively.
Based on the soil excavation activities conducted and analytical results for the over-excavation soil sample, it is
S&ME’s opinion that NCDEQ may consider closure of this incident.

Appendices

Appendix I –Figures
Z:\Shared\SME\Ops\ENV\Projects\2022\22580534_Yadkin County_Solid Waste Disposal Facility-Soil Disposal_Yadkinville, NC\4 ENV\CAD\22580534.dwgN
0 2000 4000
(IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALE
USGS TOPOGRAPHIC MAP
1149 LANDFILL ROAD
YADKINVILLE, NORTH CAROLINA
1
22580534
12-16-2022
AS SHOWN
Source : USGS Yadkinville Quadrangle, 2022.
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
SITE
Z:\Shared\SME\Ops\ENV\Projects\2022\22580534_Yadkin County_Solid Waste Disposal Facility-Soil Disposal_Yadkinville, NC\4 ENV\CAD\22580534.dwgN
SITE MAP
1149 LANDFILL ROAD
YADKINVILLE, NORTH CAROLINA
2
22580534
12-16-2022
AS SHOWN
Aerial image provided by Bing/Microsoft Corporation 2020.
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
0 200 400
(IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALE
AST LOCATION
SCALE
HOUSE
© 2022 Microsoft Corporation © 2022 Maxar ©CNES (2022) Distribution Airbus DS
SS-B SS-CAST
Z:\Shared\SME\Ops\ENV\Projects\2022\22580534_Yadkin County_Solid Waste Disposal Facility-Soil Disposal_Yadkinville, NC\4 ENV\CAD\22580534.dwgN
0 20 40
(IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALE
SOIL SAMPLE LOCATIONS
1149 LANDFILL ROAD
YADKINVILLE, NORTH CAROLINA
3
22580534
12-16-2022
AS SHOWN
Aerial image provided by Bing/Microsoft Corporation 2020.
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
LEGEND
SOIL SAMPLE LOCATION
LIMITS OF EXCAVATION
AST LOCATIONAST

Appendix II –Tables

Gasoline Range
Organics by EPA
Method by EPA Methd
8015 D
Diesel Range
Organics by EPA
Method 8015
BariumCadmiumLeadAcetophenoneBis(2-ethylhexyl) phthalatePyrene1,2,4-Trimethylbenzene2-Butanone (MEK)Acetonem-Xylene & p-XyleneTolueneGasoline Range Organics [C6-C10]Diesel Range Organics [C10-C28]Date
Collected
(mm/dd/yy)
Sample Depth
(ft bgs)
Sample
Type Sample Location mg/L mg/L mg/L mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
SS-C 12/5/22 0.5 Grab Characterization 0.237 B 0.00180 J 0.0127 J 0.0899 J 3.89 0.340 J 0.00537 J 0.0471 0.314 0.00456 J 0.0369 NA NA
SS-B 12/5/22 2.5 Grab Floor NA NA NA NA NA NA NA NA NA NA NA <3.80 12.6
---NSE 6.6 210 6.6 16 24 6 5.4 --
---NSE 47 469 156 31,200 14,000 3,120 1,250 --
---NSE 233 7,000 2,330 467,000 210,000 46,700 18,600 --
50 100
Notes:
Indicates concentration greater than Soil-to-water MSCC
Indicates concentration greater than Residential Soil Cleanup Levels
NCDEQ MSCC = Maximum Soil Contaminant Concentrations, March 7, 2022
NA = Not Analyzed
B = Compound was found in the blank sample
BGS = Below Ground Surface
mg/L = milligrams per Liter
Table 1 only includes compouns detected by the referenced laboratory analyses.
Table 1
Summary of Soil Sampling Results
Yadkin County Solid Waste Transfer Facility
1149 Landfill Road, Yadkinville, North Carolina
S&ME Project No. 22580534
mg/kg = milligrams per kilogram
Soil-to-Water MSCC (mg/kg)
Residential Soil Cleenup Levels (mg/kg)
NSEAction Level (mg/kg)
Industrial Commercial Soil Cleanup Levels (mg/kg)
J = Estimated Value NSE = No Standard Established
Sample ID
Constituent
Analytical Method RCRA 8 Metals by TCLP
Semi-Volatile Organic
Compounds by EPA Method
8270
Volitile Organic Compounds by EPA Method 8260

Appendix III- Notice of Regulatory Requirements (September 22,
2022)

September 20, 2022
Attn.: Keith Cain
1149 Landfill Road
Yadkinville, North Carolina 27055

Re: Notice of Regulatory Requirements 15A
NCAC 2L .0106(b), (c), and (f)
Corrective Action

Yadkin County Solid Waste Transfer Facility
1149 Landfill Road
Yadkin County
Incident Number: 96816
Ranking: TBD

Dear Mr. Cain:

Information received by the UST Section, Division of Waste Management, Winston-Salem Regional Office
in the Facility Compliance Inspection Report, on September 16, 2022, has been reviewed. Information in
the report confirms a release or discharge of petroleum product above ground storage tank at the above-
referenced location. This office has determined that you are responsible for the release or discharge.

As a responsible party, you must comply with the initial response and abatement action and the assessment
requirements of 15A NCAC 2L .0106(b), (c), and (f). An Initial Assessment Report prepared in accordance
with these requirements and the most recent version of the UST Section Guidelines for the Investigation
and Remediation of Contamination from Non-UST Petroleum Releases must be received by this office
within 30 days of the date of this notice. Failure to comply in the manner and time specified, may result in
the assessment of civil penalties and /or the use of other enforcement mechanisms.

Because a release or discharge has been confirmed, a Licensed Geologist or a Professional Engineer,
certified by the State of North Carolina, is required to prepare and certify all reports submitted to the
Department of Environmental Quality in accordance with Title 15A NCAC 2L .0103(e) and 2L .0111(b).

If you have any questions regarding the actions that must be taken or the rules mentioned in this letter,
please contact me at the address or telephone number listed below.

Sincerely,
Samantha Kofroth, P.G.
Hydrogeologist
Winston-Salem Regional Office
UST Section, Division of Waste Management, NCDEQ

cc: Yadkin County Health Department and Brock Hall at [e-mail]

Appendix IV- Non-Hazardous Materials Manifests

Appendix V- Analytical Laboratory Report
ANALYTICAL REPORT
PREPARED FOR
Attn: Lyndal Butler
S&ME, Inc.
8646 West Market Street
Suite 105
Greensboro, North Carolina 27409
Generated 12/20/2022 7:01:27 PM
JOB DESCRIPTION
Yadkin County Transfer Station
JOB NUMBER
680-226970-1
See page two for job notes and contact information.
Savannah GA 31404
5102 LaRoche Avenue
Eurofins Savannah
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Eurofins Savannah
Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies
Job Notes
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available. Any
exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report may not be
reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the person who
signed this report.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
Authorization
Generated
12/20/2022 7:01:27 PM
Authorized for release by
Chad Bechtold, Project Manager
[e-mail]
[phone]
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Definitions/Glossary
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Qualifiers
GC/MS VOA
Qualifier Description
*+LCS and/or LCSD is outside acceptance limits, high biased.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
S1+Surrogate recovery exceeds control limits, high biased.
GC/MS Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Metals
Qualifier Description
B Compound was found in the blank and sample.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Savannah
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Sample Summary
Client: S&ME, Inc.Job ID: 680-226970-1
Project/Site: Yadkin County Transfer Station
Lab Sample ID Client Sample ID Matrix Collected Received
680-226970-1 SS-C Solid 12/05/22 09:15 12/06/22 10:30
680-226970-2 SS-B Solid 12/05/22 09:45 12/06/22 10:30
Eurofins SavannahPage 4 of 29 12/20/2022
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Case Narrative
Client: S&ME, Inc.Job ID: 680-226970-1
Project/Site: Yadkin County Transfer Station
Job ID: 680-226970-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-226970-1
Receipt
The samples were received on 12/6/2022 10:30 AM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperature of the cooler at receipt time was 3.6°C
GC/MS VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC/MS Semi VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Gasoline Range Organics
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Diesel Range Organics
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Metals
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
General Chemistry
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
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Client Sample Results
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Lab Sample ID: 680-226970-1Client Sample ID: SS-C
Matrix: SolidDate Collected: 12/05/22 09:15
Percent Solids: 75.0Date Received: 12/06/22 10:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00688 0.00179 mg/Kg ☼12/07/22 10:03 12/11/22 21:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00688 0.00358 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND1,1,1-Trichloroethane
0.00688 0.00289 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND1,1,2,2-Tetrachloroethane
0.00688 0.00399 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00688 0.00206 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND1,1,2-Trichloroethane
0.00688 0.00399 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND1,1-Dichloroethane
0.00688 0.00495 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND1,1-Dichloroethene
0.00688 0.00275 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND1,1-Dichloropropene
0.00688 0.00275 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND1,2,3-Trichlorobenzene
0.00688 0.00248 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND1,2,3-Trichloropropane
0.00688 0.00344 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND1,2,4-Trichlorobenzene
0.00688 0.00344 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼0.00537 J1,2,4-Trimethylbenzene
0.0138 0.00220 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND1,2-Dibromo-3-Chloropropane
0.00688 0.00234 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND1,2-Dichlorobenzene
0.00688 0.00316 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND1,2-Dichloroethane
0.00688 0.00358 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND1,2-Dichloropropane
0.00688 0.00330 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND1,3,5-Trimethylbenzene
0.00688 0.00275 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND1,3-Dichlorobenzene
0.00688 0.00303 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND1,3-Dichloropropane
0.00688 0.00248 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND1,4-Dichlorobenzene
0.00688 0.00303 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND2,2-Dichloropropane
0.0344 0.0127 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼0.04712-Butanone (MEK)
0.00688 0.00316 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND2-Chlorotoluene
0.0344 0.0261 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND2-Hexanone
0.00688 0.00289 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND4-Chlorotoluene
0.00688 0.00358 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND4-Isopropyltoluene
0.0344 0.0248 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND4-Methyl-2-pentanone (MIBK)
0.0688 0.0151 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼0.314Acetone
0.00688 0.00330 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDBenzene
0.00688 0.00234 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDBromobenzene
0.00688 0.00303 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDBromoform
0.00688 0.00330 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDBromomethane
0.00688 0.00289 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼ND *+Carbon disulfide
0.00688 0.00289 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDCarbon tetrachloride
0.00688 0.00193 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDChlorobenzene
0.00688 0.00275 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDChlorobromomethane
0.00688 0.00289 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDChlorodibromomethane
0.00688 0.00303 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDChloroethane
0.00688 0.00275 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDChloroform
0.00688 0.00330 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDChloromethane
0.00688 0.00399 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDcis-1,2-Dichloroethene
0.00688 0.00303 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDcis-1,3-Dichloropropene
0.00688 0.00275 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDDibromomethane
0.00688 0.00275 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDDichlorobromomethane
0.0138 0.0138 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDEthyl acetate
0.00688 0.00289 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDEthylbenzene
0.00688 0.00234 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDEthylene Dibromide
0.00688 0.00564 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDHexachlorobutadiene
0.00688 0.00234 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDHexane
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Client Sample Results
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Lab Sample ID: 680-226970-1Client Sample ID: SS-C
Matrix: SolidDate Collected: 12/05/22 09:15
Percent Solids: 75.0Date Received: 12/06/22 10:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 0.00688 0.00234 mg/Kg ☼12/07/22 10:03 12/11/22 21:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0138 0.00206 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDIsopropyl ether
0.00688 0.00303 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDIsopropylbenzene
0.00688 0.00303 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDMethyl tert-butyl ether
0.0138 0.0110 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDMethylene Chloride
0.00688 0.00303 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼0.00456 Jm-Xylene & p-Xylene
0.00688 0.00426 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDNaphthalene
0.00688 0.00261 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDn-Butylbenzene
0.00688 0.00592 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDn-Heptane
0.00688 0.00303 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDN-Propylbenzene
0.00688 0.00316 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDo-Xylene
0.00688 0.00275 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDsec-Butylbenzene
0.00688 0.00261 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDStyrene
0.00688 0.00344 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDtert-Butylbenzene
0.00688 0.00358 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDTetrachloroethene
0.00688 0.00358 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼0.0369Toluene
0.00688 0.00316 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDtrans-1,2-Dichloroethene
0.00688 0.00358 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDtrans-1,3-Dichloropropene
0.0138 0.00330 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDtrans-1,4-Dichloro-2-butene
0.00688 0.00248 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDTrichloroethene
0.00688 0.00426 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDTrichlorofluoromethane
0.0138 0.00757 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDVinyl acetate
0.00688 0.00385 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDVinyl chloride
0.0138 0.00495 mg/Kg 12/07/22 10:03 12/11/22 21:39 1☼NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)105 65-130 12/07/22 10:03 12/11/22 21:39 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)136 S1+12/07/22 10:03 12/11/22 21:39 165-130
Dibromofluoromethane (Surr)113 12/07/22 10:03 12/11/22 21:39 165-130
Toluene-d8 (Surr)110 12/07/22 10:03 12/11/22 21:39 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 2.18 2.18 mg/Kg ☼12/09/22 11:25 12/12/22 06:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.423 0.0448 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND2,4,5-Trichlorophenol
0.423 0.0372 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND2,4,6-Trichlorophenol
0.423 0.0448 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND2,4-Dichlorophenol
0.423 0.0564 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND2,4-Dimethylphenol
2.18 1.06 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND2,4-Dinitrophenol
0.423 0.0628 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND2,4-Dinitrotoluene
0.423 0.0538 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND2,6-Dinitrotoluene
0.423 0.0448 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND2-Chloronaphthalene
0.423 0.0512 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND2-Chlorophenol
0.423 0.0487 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND2-Methylnaphthalene
0.423 0.0346 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND2-Methylphenol
2.18 0.0577 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND2-Nitroaniline
0.423 0.0525 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND2-Nitrophenol
0.423 0.0551 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND3 & 4 Methylphenol
0.846 0.0359 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND3,3'-Dichlorobenzidine
2.18 0.0589 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Lab Sample ID: 680-226970-1Client Sample ID: SS-C
Matrix: SolidDate Collected: 12/05/22 09:15
Percent Solids: 75.0Date Received: 12/06/22 10:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 2.18 0.218 mg/Kg ☼12/09/22 11:25 12/12/22 06:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.423 0.0461 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND4-Bromophenyl phenyl ether
0.423 0.0448 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND4-Chloro-3-methylphenol
0.846 0.0666 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND4-Chloroaniline
0.423 0.0564 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND4-Chlorophenyl phenyl ether
2.18 0.0628 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND4-Nitroaniline
2.18 0.423 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼ND4-Nitrophenol
0.423 0.0525 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDAcenaphthene
0.423 0.0461 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDAcenaphthylene
0.423 0.0359 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼0.0899 JAcetophenone
0.423 0.0320 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDAnthracene
0.423 0.0295 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDAtrazine
0.423 0.0743 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDBenzaldehyde
0.423 0.0346 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDBenzo[a]anthracene
0.423 0.0666 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDBenzo[a]pyrene
0.423 0.0487 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDBenzo[b]fluoranthene
0.423 0.0282 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDBenzo[g,h,i]perylene
0.423 0.0833 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDBenzo[k]fluoranthene
0.423 0.0384 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDbis (2-chloroisopropyl) ether
0.423 0.0500 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDBis(2-chloroethoxy)methane
0.423 0.0577 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDBis(2-chloroethyl)ether
0.423 0.0372 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼3.89Bis(2-ethylhexyl) phthalate
0.423 0.0333 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDButyl benzyl phthalate
0.423 0.0846 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDCaprolactam
0.423 0.0384 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDCarbazole
0.423 0.0269 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDChrysene
0.423 0.0500 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDDibenz(a,h)anthracene
0.423 0.0423 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDDibenzofuran
0.423 0.0474 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDDiethyl phthalate
0.423 0.0436 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDDimethyl phthalate
0.423 0.0384 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDDi-n-butyl phthalate
0.423 0.0372 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDDi-n-octyl phthalate
0.423 0.0410 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDFluoranthene
0.423 0.0461 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDFluorene
0.423 0.0500 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDHexachlorobenzene
0.423 0.0461 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDHexachlorobutadiene
0.423 0.0525 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDHexachlorocyclopentadiene
0.423 0.0359 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDHexachloroethane
0.423 0.0359 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDIndeno[1,2,3-cd]pyrene
0.423 0.0423 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDIsophorone
0.423 0.0384 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDNaphthalene
0.423 0.0333 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDNitrobenzene
0.423 0.0410 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDN-Nitrosodi-n-propylamine
0.423 0.0423 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDN-Nitrosodiphenylamine
2.18 0.423 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDPentachlorophenol
0.423 0.0346 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDPhenanthrene
0.423 0.0436 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼NDPhenol
0.423 0.0346 mg/Kg 12/09/22 11:25 12/12/22 06:26 1☼0.340 JPyrene
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Client Sample Results
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Lab Sample ID: 680-226970-1Client Sample ID: SS-C
Matrix: SolidDate Collected: 12/05/22 09:15
Percent Solids: 75.0Date Received: 12/06/22 10:30
2,4,6-Tribromophenol (Surr)42 21-132 12/09/22 11:25 12/12/22 06:26 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)38 12/09/22 11:25 12/12/22 06:26 125-130
2-Fluorophenol (Surr)30 12/09/22 11:25 12/12/22 06:26 118-130
Nitrobenzene-d5 (Surr)31 12/09/22 11:25 12/12/22 06:26 119-130
Phenol-d5 (Surr)33 12/09/22 11:25 12/12/22 06:26 121-130
Terphenyl-d14 (Surr)44 12/09/22 11:25 12/12/22 06:26 131-133
Method: SW846 6020B - Metals (ICP/MS) - TCLP
RL MDL
ND 0.0300 0.00860 mg/L 12/14/22 05:07 12/14/22 18:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Arsenic
0.0500 0.00890 mg/L 12/14/22 05:07 12/14/22 18:50 10.237 BBarium
0.00500 0.000780 mg/L 12/14/22 05:07 12/14/22 18:50 10.00180 JCadmium
0.0500 0.0260 mg/L 12/14/22 05:07 12/14/22 18:50 1NDChromium
0.0250 0.00340 mg/L 12/14/22 05:07 12/14/22 18:50 10.0127 JLead
0.0250 0.0120 mg/L 12/14/22 05:07 12/14/22 18:50 1NDSelenium
0.0100 0.00390 mg/L 12/14/22 05:07 12/14/22 18:50 1NDSilver
Method: SW846 7470A - Mercury (CVAA) - TCLP
RL MDL
ND 0.0200 0.0200 mg/L 12/14/22 07:33 12/14/22 17:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Mercury
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Client Sample Results
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Lab Sample ID: 680-226970-2Client Sample ID: SS-B
Matrix: SolidDate Collected: 12/05/22 09:45
Percent Solids: 76.2Date Received: 12/06/22 10:30
Method: SW846 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 15.2 3.80 mg/Kg ☼12/07/22 10:03 12/16/22 16:35 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene 77 70-131 12/07/22 10:03 12/16/22 16:35 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
12.6 10.4 3.39 mg/Kg ☼12/08/22 18:10 12/09/22 21:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 40 15-139 12/08/22 18:10 12/09/22 21:59 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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QC Sample Results
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Method: 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 680-754573/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754573
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00500 0.00130 mg/Kg 12/11/22 13:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002600.00500 mg/Kg 12/11/22 13:24 11,1,1-Trichloroethane
ND 0.002100.00500 mg/Kg 12/11/22 13:24 11,1,2,2-Tetrachloroethane
ND 0.002900.00500 mg/Kg 12/11/22 13:24 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.001500.00500 mg/Kg 12/11/22 13:24 11,1,2-Trichloroethane
ND 0.002900.00500 mg/Kg 12/11/22 13:24 11,1-Dichloroethane
ND 0.003600.00500 mg/Kg 12/11/22 13:24 11,1-Dichloroethene
ND 0.002000.00500 mg/Kg 12/11/22 13:24 11,1-Dichloropropene
ND 0.002000.00500 mg/Kg 12/11/22 13:24 11,2,3-Trichlorobenzene
ND 0.001800.00500 mg/Kg 12/11/22 13:24 11,2,3-Trichloropropane
ND 0.002500.00500 mg/Kg 12/11/22 13:24 11,2,4-Trichlorobenzene
ND 0.002500.00500 mg/Kg 12/11/22 13:24 11,2,4-Trimethylbenzene
ND 0.001600.0100 mg/Kg 12/11/22 13:24 11,2-Dibromo-3-Chloropropane
ND 0.001700.00500 mg/Kg 12/11/22 13:24 11,2-Dichlorobenzene
ND 0.002300.00500 mg/Kg 12/11/22 13:24 11,2-Dichloroethane
ND 0.002600.00500 mg/Kg 12/11/22 13:24 11,2-Dichloropropane
ND 0.002400.00500 mg/Kg 12/11/22 13:24 11,3,5-Trimethylbenzene
ND 0.002000.00500 mg/Kg 12/11/22 13:24 11,3-Dichlorobenzene
ND 0.002200.00500 mg/Kg 12/11/22 13:24 11,3-Dichloropropane
ND 0.001800.00500 mg/Kg 12/11/22 13:24 11,4-Dichlorobenzene
ND 0.002200.00500 mg/Kg 12/11/22 13:24 12,2-Dichloropropane
ND 0.009200.0250 mg/Kg 12/11/22 13:24 12-Butanone (MEK)
ND 0.002300.00500 mg/Kg 12/11/22 13:24 12-Chlorotoluene
ND 0.01900.0250 mg/Kg 12/11/22 13:24 12-Hexanone
ND 0.002100.00500 mg/Kg 12/11/22 13:24 14-Chlorotoluene
ND 0.002600.00500 mg/Kg 12/11/22 13:24 14-Isopropyltoluene
ND 0.01800.0250 mg/Kg 12/11/22 13:24 14-Methyl-2-pentanone (MIBK)
ND 0.01100.0500 mg/Kg 12/11/22 13:24 1Acetone
ND 0.002400.00500 mg/Kg 12/11/22 13:24 1Benzene
ND 0.001700.00500 mg/Kg 12/11/22 13:24 1Bromobenzene
ND 0.002200.00500 mg/Kg 12/11/22 13:24 1Bromoform
ND 0.002400.00500 mg/Kg 12/11/22 13:24 1Bromomethane
ND 0.002100.00500 mg/Kg 12/11/22 13:24 1Carbon disulfide
ND 0.002100.00500 mg/Kg 12/11/22 13:24 1Carbon tetrachloride
ND 0.001400.00500 mg/Kg 12/11/22 13:24 1Chlorobenzene
ND 0.002000.00500 mg/Kg 12/11/22 13:24 1Chlorobromomethane
ND 0.002100.00500 mg/Kg 12/11/22 13:24 1Chlorodibromomethane
ND 0.002200.00500 mg/Kg 12/11/22 13:24 1Chloroethane
ND 0.002000.00500 mg/Kg 12/11/22 13:24 1Chloroform
ND 0.002400.00500 mg/Kg 12/11/22 13:24 1Chloromethane
ND 0.002900.00500 mg/Kg 12/11/22 13:24 1cis-1,2-Dichloroethene
ND 0.002200.00500 mg/Kg 12/11/22 13:24 1cis-1,3-Dichloropropene
ND 0.002000.00500 mg/Kg 12/11/22 13:24 1Dibromomethane
ND 0.002000.00500 mg/Kg 12/11/22 13:24 1Dichlorobromomethane
ND 0.01000.0100 mg/Kg 12/11/22 13:24 1Ethyl acetate
ND 0.002100.00500 mg/Kg 12/11/22 13:24 1Ethylbenzene
ND 0.001700.00500 mg/Kg 12/11/22 13:24 1Ethylene Dibromide
ND 0.004100.00500 mg/Kg 12/11/22 13:24 1Hexachlorobutadiene
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QC Sample Results
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-754573/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754573
RL MDL
Hexane ND 0.00500 0.00170 mg/Kg 12/11/22 13:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.001700.00500 mg/Kg 12/11/22 13:24 1Iodomethane
ND 0.001500.0100 mg/Kg 12/11/22 13:24 1Isopropyl ether
ND 0.002200.00500 mg/Kg 12/11/22 13:24 1Isopropylbenzene
ND 0.002200.00500 mg/Kg 12/11/22 13:24 1Methyl tert-butyl ether
ND 0.008000.0100 mg/Kg 12/11/22 13:24 1Methylene Chloride
ND 0.002200.00500 mg/Kg 12/11/22 13:24 1m-Xylene & p-Xylene
ND 0.003100.00500 mg/Kg 12/11/22 13:24 1Naphthalene
ND 0.001900.00500 mg/Kg 12/11/22 13:24 1n-Butylbenzene
ND 0.004300.00500 mg/Kg 12/11/22 13:24 1n-Heptane
ND 0.002200.00500 mg/Kg 12/11/22 13:24 1N-Propylbenzene
ND 0.002300.00500 mg/Kg 12/11/22 13:24 1o-Xylene
ND 0.002000.00500 mg/Kg 12/11/22 13:24 1sec-Butylbenzene
ND 0.001900.00500 mg/Kg 12/11/22 13:24 1Styrene
ND 0.002500.00500 mg/Kg 12/11/22 13:24 1tert-Butylbenzene
ND 0.002600.00500 mg/Kg 12/11/22 13:24 1Tetrachloroethene
ND 0.002600.00500 mg/Kg 12/11/22 13:24 1Toluene
ND 0.002300.00500 mg/Kg 12/11/22 13:24 1trans-1,2-Dichloroethene
ND 0.002600.00500 mg/Kg 12/11/22 13:24 1trans-1,3-Dichloropropene
ND 0.002400.0100 mg/Kg 12/11/22 13:24 1trans-1,4-Dichloro-2-butene
ND 0.001800.00500 mg/Kg 12/11/22 13:24 1Trichloroethene
ND 0.003100.00500 mg/Kg 12/11/22 13:24 1Trichlorofluoromethane
ND 0.005500.0100 mg/Kg 12/11/22 13:24 1Vinyl acetate
ND 0.002800.00500 mg/Kg 12/11/22 13:24 1Vinyl chloride
ND 0.003600.0100 mg/Kg 12/11/22 13:24 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)89 65-130 12/11/22 13:24 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
93 12/11/22 13:24 14-Bromofluorobenzene (Surr)65-130
102 12/11/22 13:24 1Dibromofluoromethane (Surr)65-130
105 12/11/22 13:24 1Toluene-d8 (Surr)65-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-754573/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754573
1,1,1,2-Tetrachloroethane 0.0500 0.05413 mg/Kg 108 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 0.0500 0.05241 mg/Kg 105 70 -130
1,1,2,2-Tetrachloroethane 0.0500 0.04824 mg/Kg 96 64 -130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.06153 mg/Kg 123 70 -130
1,1,2-Trichloroethane 0.0500 0.04850 mg/Kg 97 56 -146
1,1-Dichloroethane 0.0500 0.04965 mg/Kg 99 70 -130
1,1-Dichloroethene 0.0500 0.05879 mg/Kg 118 69 -130
1,1-Dichloropropene 0.0500 0.05228 mg/Kg 105 70 -130
1,2,3-Trichlorobenzene 0.0500 0.04988 mg/Kg 100 70 -130
1,2,3-Trichloropropane 0.0500 0.05089 mg/Kg 102 64 -130
1,2,4-Trichlorobenzene 0.0500 0.05238 mg/Kg 105 70 -130
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QC Sample Results
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-754573/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754573
1,2,4-Trimethylbenzene 0.0500 0.05500 mg/Kg 110 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,2-Dibromo-3-Chloropropane 0.0500 0.04376 mg/Kg 88 42 -145
1,2-Dichlorobenzene 0.0500 0.05197 mg/Kg 104 70 -130
1,2-Dichloroethane 0.0500 0.04912 mg/Kg 98 68 -139
1,2-Dichloropropane 0.0500 0.04854 mg/Kg 97 70 -130
1,3,5-Trimethylbenzene 0.0500 0.05488 mg/Kg 110 70 -130
1,3-Dichlorobenzene 0.0500 0.05213 mg/Kg 104 70 -130
1,3-Dichloropropane 0.0500 0.05055 mg/Kg 101 54 -150
1,4-Dichlorobenzene 0.0500 0.05213 mg/Kg 104 70 -130
2,2-Dichloropropane 0.0500 0.05133 mg/Kg 103 70 -130
2-Butanone (MEK)0.250 0.2023 mg/Kg 81 40 -150
2-Chlorotoluene 0.0500 0.05273 mg/Kg 105 70 -130
2-Hexanone 0.250 0.2020 mg/Kg 81 30 -150
4-Chlorotoluene 0.0500 0.04776 mg/Kg 96 70 -130
4-Isopropyltoluene 0.0500 0.04924 mg/Kg 98 70 -130
4-Methyl-2-pentanone (MIBK)0.250 0.2075 mg/Kg 83 34 -150
Acetone 0.250 0.2041 mg/Kg 82 10 -150
Benzene 0.0500 0.05306 mg/Kg 106 70 -130
Bromobenzene 0.0500 0.05805 mg/Kg 116 70 -130
Bromoform 0.0500 0.05188 mg/Kg 104 68 -130
Bromomethane 0.0500 0.05809 mg/Kg 116 70 -130
Carbon disulfide 0.0500 0.06554 *+mg/Kg 131 70 -130
Carbon tetrachloride 0.0500 0.05397 mg/Kg 108 70 -130
Chlorobenzene 0.0500 0.05554 mg/Kg 111 70 -130
Chlorobromomethane 0.0500 0.05772 mg/Kg 115 66 -130
Chlorodibromomethane 0.0500 0.05168 mg/Kg 103 64 -133
Chloroethane 0.0500 0.05385 mg/Kg 108 70 -130
Chloroform 0.0500 0.05033 mg/Kg 101 70 -130
Chloromethane 0.0500 0.04614 mg/Kg 92 70 -130
cis-1,2-Dichloroethene 0.0500 0.04955 mg/Kg 99 70 -130
cis-1,3-Dichloropropene 0.0500 0.04848 mg/Kg 97 70 -130
Dibromomethane 0.0500 0.05351 mg/Kg 107 59 -142
Dichlorobromomethane 0.0500 0.04886 mg/Kg 98 70 -130
Ethylbenzene 0.0500 0.05326 mg/Kg 107 70 -130
Ethylene Dibromide 0.0500 0.05325 mg/Kg 106 48 -150
Hexachlorobutadiene 0.0500 0.05655 mg/Kg 113 70 -130
Hexane 0.0500 0.05633 mg/Kg 113 70 -130
Iodomethane 0.0500 0.05786 mg/Kg 116 65 -138
Isopropylbenzene 0.0500 0.05543 mg/Kg 111 70 -130
Methyl tert-butyl ether 0.0500 0.05024 mg/Kg 100 70 -130
Methylene Chloride 0.0500 0.05441 mg/Kg 109 54 -149
m-Xylene & p-Xylene 0.0500 0.05190 mg/Kg 104 70 -130
Naphthalene 0.0500 0.04565 mg/Kg 91 46 -150
n-Butylbenzene 0.0500 0.04788 mg/Kg 96 70 -130
n-Heptane 0.0500 0.05251 mg/Kg 105 70 -130
N-Propylbenzene 0.0500 0.05351 mg/Kg 107 70 -130
o-Xylene 0.0500 0.05302 mg/Kg 106 70 -130
sec-Butylbenzene 0.0500 0.05475 mg/Kg 109 69 -142
Styrene 0.0500 0.05484 mg/Kg 110 70 -130
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QC Sample Results
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-754573/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754573
tert-Butylbenzene 0.0500 0.05592 mg/Kg 112 67 -145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Tetrachloroethene 0.0500 0.06096 mg/Kg 122 70 -130
Toluene 0.0500 0.05411 mg/Kg 108 70 -130
trans-1,2-Dichloroethene 0.0500 0.05486 mg/Kg 110 67 -130
trans-1,3-Dichloropropene 0.0500 0.04967 mg/Kg 99 54 -150
trans-1,4-Dichloro-2-butene 0.0500 0.04473 mg/Kg 89 54 -150
Trichloroethene 0.0500 0.05621 mg/Kg 112 70 -130
Trichlorofluoromethane 0.0500 0.05982 mg/Kg 120 70 -130
Vinyl acetate 0.100 0.07599 mg/Kg 76 53 -150
Vinyl chloride 0.0500 0.05100 mg/Kg 102 70 -130
Xylenes, Total 0.100 0.1049 mg/Kg 105 70 -130
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
103
LCS LCS
Qualifier Limits%Recovery
934-Bromofluorobenzene (Surr)65 -130
107Dibromofluoromethane (Surr)65 -130
106Toluene-d8 (Surr)65 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-754573/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754573
1,1,1,2-Tetrachloroethane 0.0500 0.05523 mg/Kg 110 70 -130 2 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 0.0500 0.05274 mg/Kg 105 70 -130 1 30
1,1,2,2-Tetrachloroethane 0.0500 0.04708 mg/Kg 94 64 -130 2 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.06112 mg/Kg 122 70 -130 1 40
1,1,2-Trichloroethane 0.0500 0.04720 mg/Kg 94 56 -146 3 30
1,1-Dichloroethane 0.0500 0.04993 mg/Kg 100 70 -130 1 30
1,1-Dichloroethene 0.0500 0.05920 mg/Kg 118 69 -130 1 50
1,1-Dichloropropene 0.0500 0.05253 mg/Kg 105 70 -130 0 30
1,2,3-Trichlorobenzene 0.0500 0.04981 mg/Kg 100 70 -130 0 30
1,2,3-Trichloropropane 0.0500 0.04973 mg/Kg 99 64 -130 2 30
1,2,4-Trichlorobenzene 0.0500 0.05257 mg/Kg 105 70 -130 0 30
1,2,4-Trimethylbenzene 0.0500 0.05439 mg/Kg 109 70 -130 1 30
1,2-Dibromo-3-Chloropropane 0.0500 0.04389 mg/Kg 88 42 -145 0 30
1,2-Dichlorobenzene 0.0500 0.05188 mg/Kg 104 70 -130 0 30
1,2-Dichloroethane 0.0500 0.04885 mg/Kg 98 68 -139 1 30
1,2-Dichloropropane 0.0500 0.04853 mg/Kg 97 70 -130 0 30
1,3,5-Trimethylbenzene 0.0500 0.05543 mg/Kg 111 70 -130 1 30
1,3-Dichlorobenzene 0.0500 0.05275 mg/Kg 106 70 -130 1 30
1,3-Dichloropropane 0.0500 0.04827 mg/Kg 97 54 -150 5 30
1,4-Dichlorobenzene 0.0500 0.05223 mg/Kg 104 70 -130 0 30
2,2-Dichloropropane 0.0500 0.05151 mg/Kg 103 70 -130 0 30
2-Butanone (MEK)0.250 0.1999 mg/Kg 80 40 -150 1 30
2-Chlorotoluene 0.0500 0.05235 mg/Kg 105 70 -130 1 30
2-Hexanone 0.250 0.1991 mg/Kg 80 30 -150 1 30
4-Chlorotoluene 0.0500 0.04802 mg/Kg 96 70 -130 1 30
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QC Sample Results
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-754573/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754573
4-Isopropyltoluene 0.0500 0.05024 mg/Kg 100 70 -130 2 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
4-Methyl-2-pentanone (MIBK)0.250 0.2025 mg/Kg 81 34 -150 2 30
Acetone 0.250 0.2101 mg/Kg 84 10 -150 3 50
Benzene 0.0500 0.05294 mg/Kg 106 70 -130 0 30
Bromobenzene 0.0500 0.05763 mg/Kg 115 70 -130 1 30
Bromoform 0.0500 0.05136 mg/Kg 103 68 -130 1 30
Bromomethane 0.0500 0.05718 mg/Kg 114 70 -130 2 30
Carbon disulfide 0.0500 0.06616 *+mg/Kg 132 70 -130 1 30
Carbon tetrachloride 0.0500 0.05444 mg/Kg 109 70 -130 1 30
Chlorobenzene 0.0500 0.05586 mg/Kg 112 70 -130 1 30
Chlorobromomethane 0.0500 0.05672 mg/Kg 113 66 -130 2 30
Chlorodibromomethane 0.0500 0.05056 mg/Kg 101 64 -133 2 30
Chloroethane 0.0500 0.05215 mg/Kg 104 70 -130 3 30
Chloroform 0.0500 0.05031 mg/Kg 101 70 -130 0 30
Chloromethane 0.0500 0.04525 mg/Kg 90 70 -130 2 30
cis-1,2-Dichloroethene 0.0500 0.04971 mg/Kg 99 70 -130 0 30
cis-1,3-Dichloropropene 0.0500 0.04860 mg/Kg 97 70 -130 0 30
Dibromomethane 0.0500 0.05158 mg/Kg 103 59 -142 4 30
Dichlorobromomethane 0.0500 0.04843 mg/Kg 97 70 -130 1 30
Ethylbenzene 0.0500 0.05376 mg/Kg 108 70 -130 1 30
Ethylene Dibromide 0.0500 0.05180 mg/Kg 104 48 -150 3 30
Hexachlorobutadiene 0.0500 0.05798 mg/Kg 116 70 -130 2 30
Hexane 0.0500 0.05438 mg/Kg 109 70 -130 4 30
Iodomethane 0.0500 0.05748 mg/Kg 115 65 -138 1 30
Isopropylbenzene 0.0500 0.05569 mg/Kg 111 70 -130 0 30
Methyl tert-butyl ether 0.0500 0.04851 mg/Kg 97 70 -130 4 30
Methylene Chloride 0.0500 0.05385 mg/Kg 108 54 -149 1 30
m-Xylene & p-Xylene 0.0500 0.05333 mg/Kg 107 70 -130 3 30
Naphthalene 0.0500 0.04521 mg/Kg 90 46 -150 1 30
n-Butylbenzene 0.0500 0.04852 mg/Kg 97 70 -130 1 30
n-Heptane 0.0500 0.05210 mg/Kg 104 70 -130 1 30
N-Propylbenzene 0.0500 0.05379 mg/Kg 108 70 -130 1 30
o-Xylene 0.0500 0.05279 mg/Kg 106 70 -130 0 30
sec-Butylbenzene 0.0500 0.05537 mg/Kg 111 69 -142 1 30
Styrene 0.0500 0.05516 mg/Kg 110 70 -130 1 30
tert-Butylbenzene 0.0500 0.05592 mg/Kg 112 67 -145 0 30
Tetrachloroethene 0.0500 0.06132 mg/Kg 123 70 -130 1 30
Toluene 0.0500 0.05432 mg/Kg 109 70 -130 0 30
trans-1,2-Dichloroethene 0.0500 0.05520 mg/Kg 110 67 -130 1 30
trans-1,3-Dichloropropene 0.0500 0.04841 mg/Kg 97 54 -150 3 30
trans-1,4-Dichloro-2-butene 0.0500 0.04451 mg/Kg 89 54 -150 0 30
Trichloroethene 0.0500 0.05644 mg/Kg 113 70 -130 0 30
Trichlorofluoromethane 0.0500 0.05814 mg/Kg 116 70 -130 3 30
Vinyl acetate 0.100 0.07295 mg/Kg 73 53 -150 4 30
Vinyl chloride 0.0500 0.04934 mg/Kg 99 70 -130 3 30
Xylenes, Total 0.100 0.1061 mg/Kg 106 70 -130 1 30
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QC Sample Results
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-754573/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754573
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
95
LCSD LCSD
Qualifier Limits%Recovery
944-Bromofluorobenzene (Surr)65 -130
106Dibromofluoromethane (Surr)65 -130
106Toluene-d8 (Surr)65 -130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-754395/13-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754609 Prep Batch: 754395
RL MDL
1,1'-Biphenyl ND 1.61 1.61 mg/Kg 12/09/22 11:25 12/11/22 21:48 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.03310.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 12,4,5-Trichlorophenol
ND 0.02750.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 12,4,6-Trichlorophenol
ND 0.03310.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 12,4-Dichlorophenol
ND 0.04170.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 12,4-Dimethylphenol
ND 0.7861.61 mg/Kg 12/09/22 11:25 12/11/22 21:48 12,4-Dinitrophenol
ND 0.04640.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 12,4-Dinitrotoluene
ND 0.03980.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 12,6-Dinitrotoluene
ND 0.03310.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 12-Chloronaphthalene
ND 0.03790.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 12-Chlorophenol
ND 0.03600.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 12-Methylnaphthalene
ND 0.02560.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 12-Methylphenol
ND 0.04261.61 mg/Kg 12/09/22 11:25 12/11/22 21:48 12-Nitroaniline
ND 0.03880.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 12-Nitrophenol
ND 0.04070.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 13 & 4 Methylphenol
ND 0.02650.625 mg/Kg 12/09/22 11:25 12/11/22 21:48 13,3'-Dichlorobenzidine
ND 0.04361.61 mg/Kg 12/09/22 11:25 12/11/22 21:48 13-Nitroaniline
ND 0.1611.61 mg/Kg 12/09/22 11:25 12/11/22 21:48 14,6-Dinitro-2-methylphenol
ND 0.03410.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 14-Bromophenyl phenyl ether
ND 0.03310.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 14-Chloro-3-methylphenol
ND 0.04920.625 mg/Kg 12/09/22 11:25 12/11/22 21:48 14-Chloroaniline
ND 0.04170.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 14-Chlorophenyl phenyl ether
ND 0.04641.61 mg/Kg 12/09/22 11:25 12/11/22 21:48 14-Nitroaniline
ND 0.3131.61 mg/Kg 12/09/22 11:25 12/11/22 21:48 14-Nitrophenol
ND 0.03880.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Acenaphthene
ND 0.03410.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Acenaphthylene
ND 0.02650.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Acetophenone
ND 0.02370.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Anthracene
ND 0.02180.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Atrazine
ND 0.05490.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Benzaldehyde
ND 0.02560.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Benzo[a]anthracene
ND 0.04920.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Benzo[a]pyrene
ND 0.03600.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Benzo[b]fluoranthene
ND 0.02080.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Benzo[g,h,i]perylene
ND 0.06160.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Benzo[k]fluoranthene
ND 0.02840.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1bis (2-chloroisopropyl) ether
ND 0.03690.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Bis(2-chloroethoxy)methane
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QC Sample Results
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-754395/13-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754609 Prep Batch: 754395
RL MDL
Bis(2-chloroethyl)ether ND 0.313 0.0426 mg/Kg 12/09/22 11:25 12/11/22 21:48 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.02750.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Bis(2-ethylhexyl) phthalate
ND 0.02460.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Butyl benzyl phthalate
ND 0.06250.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Caprolactam
ND 0.02840.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Carbazole
ND 0.01990.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Chrysene
ND 0.03690.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Dibenz(a,h)anthracene
ND 0.03130.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Dibenzofuran
ND 0.03500.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Diethyl phthalate
ND 0.03220.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Dimethyl phthalate
ND 0.02840.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Di-n-butyl phthalate
ND 0.02750.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Di-n-octyl phthalate
ND 0.03030.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Fluoranthene
ND 0.03410.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Fluorene
ND 0.03690.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Hexachlorobenzene
ND 0.03410.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Hexachlorobutadiene
ND 0.03880.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Hexachlorocyclopentadiene
ND 0.02650.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Hexachloroethane
ND 0.02650.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Indeno[1,2,3-cd]pyrene
ND 0.03130.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Isophorone
ND 0.02840.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Naphthalene
ND 0.02460.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Nitrobenzene
ND 0.03030.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1N-Nitrosodi-n-propylamine
ND 0.03130.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1N-Nitrosodiphenylamine
ND 0.3131.61 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Pentachlorophenol
ND 0.02560.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Phenanthrene
ND 0.03220.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Phenol
ND 0.02560.313 mg/Kg 12/09/22 11:25 12/11/22 21:48 1Pyrene
2,4,6-Tribromophenol (Surr)99 21-132 12/11/22 21:48 1
MB MB
Surrogate
12/09/22 11:25
Dil FacPreparedAnalyzedQualifierLimits%Recovery
79 12/09/22 11:25 12/11/22 21:48 12-Fluorobiphenyl (Surr)25-130
73 12/09/22 11:25 12/11/22 21:48 12-Fluorophenol (Surr)18-130
70 12/09/22 11:25 12/11/22 21:48 1Nitrobenzene-d5 (Surr)19-130
75 12/09/22 11:25 12/11/22 21:48 1Phenol-d5 (Surr)21-130
100 12/09/22 11:25 12/11/22 21:48 1Terphenyl-d14 (Surr)31-133
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-754395/14-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754609 Prep Batch: 754395
1,1'-Biphenyl 6.54 4.820 mg/Kg 74 32 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2,4,5-Trichlorophenol 6.54 5.370 mg/Kg 82 33 -130
2,4,6-Trichlorophenol 6.54 5.450 mg/Kg 83 31 -130
2,4-Dichlorophenol 6.54 5.202 mg/Kg 80 30 -130
2,4-Dimethylphenol 6.54 5.010 mg/Kg 77 34 -130
2,4-Dinitrophenol 13.1 13.74 mg/Kg 105 10 -130
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QC Sample Results
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-754395/14-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754609 Prep Batch: 754395
2,4-Dinitrotoluene 6.54 6.524 mg/Kg 100 34 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2,6-Dinitrotoluene 6.54 5.961 mg/Kg 91 33 -130
2-Chloronaphthalene 6.54 4.817 mg/Kg 74 30 -130
2-Chlorophenol 6.54 4.837 mg/Kg 74 28 -130
2-Methylnaphthalene 6.54 4.636 mg/Kg 71 28 -130
2-Methylphenol 6.54 4.867 mg/Kg 74 30 -130
2-Nitroaniline 6.54 6.200 mg/Kg 95 26 -130
2-Nitrophenol 6.54 5.435 mg/Kg 83 24 -130
3 & 4 Methylphenol 6.54 4.984 mg/Kg 76 31 -130
3,3'-Dichlorobenzidine 6.54 5.795 mg/Kg 89 10 -130
3-Nitroaniline 6.54 5.672 mg/Kg 87 10 -130
4,6-Dinitro-2-methylphenol 13.1 13.67 mg/Kg 105 22 -130
4-Bromophenyl phenyl ether 6.54 4.975 mg/Kg 76 32 -130
4-Chloro-3-methylphenol 6.54 5.848 mg/Kg 89 31 -130
4-Chloroaniline 6.54 3.766 mg/Kg 58 10 -130
4-Chlorophenyl phenyl ether 6.54 5.308 mg/Kg 81 32 -130
4-Nitroaniline 6.54 6.144 mg/Kg 94 25 -130
4-Nitrophenol 13.1 12.76 mg/Kg 98 25 -130
Acenaphthene 6.54 5.380 mg/Kg 82 33 -130
Acenaphthylene 6.54 5.209 mg/Kg 80 34 -130
Acetophenone 6.54 4.611 mg/Kg 71 28 -130
Anthracene 6.54 5.216 mg/Kg 80 39 -130
Atrazine 6.54 5.700 mg/Kg 87 27 -130
Benzaldehyde 6.54 4.777 mg/Kg 73 10 -130
Benzo[a]anthracene 6.54 5.975 mg/Kg 91 40 -130
Benzo[a]pyrene 6.54 5.174 mg/Kg 79 37 -131
Benzo[b]fluoranthene 6.54 5.113 mg/Kg 78 35 -130
Benzo[g,h,i]perylene 6.54 5.283 mg/Kg 81 39 -130
Benzo[k]fluoranthene 6.54 5.108 mg/Kg 78 35 -130
bis (2-chloroisopropyl) ether 6.54 4.752 mg/Kg 73 12 -130
Bis(2-chloroethoxy)methane 6.54 4.812 mg/Kg 74 29 -130
Bis(2-chloroethyl)ether 6.54 4.141 mg/Kg 63 18 -130
Bis(2-ethylhexyl) phthalate 6.54 6.314 mg/Kg 97 39 -130
Butyl benzyl phthalate 6.54 6.822 mg/Kg 104 38 -130
Caprolactam 6.54 6.388 mg/Kg 98 27 -148
Carbazole 6.54 5.399 mg/Kg 83 43 -130
Chrysene 6.54 5.534 mg/Kg 85 40 -130
Dibenz(a,h)anthracene 6.54 5.183 mg/Kg 79 37 -130
Dibenzofuran 6.54 5.158 mg/Kg 79 34 -130
Diethyl phthalate 6.54 5.638 mg/Kg 86 36 -130
Dimethyl phthalate 6.54 5.389 mg/Kg 82 36 -130
Di-n-butyl phthalate 6.54 5.734 mg/Kg 88 39 -130
Di-n-octyl phthalate 6.54 7.124 mg/Kg 109 38 -131
Fluoranthene 6.54 5.500 mg/Kg 84 38 -130
Fluorene 6.54 5.284 mg/Kg 81 34 -130
Hexachlorobenzene 6.54 4.992 mg/Kg 76 28 -130
Hexachlorobutadiene 6.54 4.330 mg/Kg 66 22 -130
Hexachlorocyclopentadiene 6.54 4.333 mg/Kg 66 11 -130
Hexachloroethane 6.54 4.121 mg/Kg 63 21 -130
Eurofins Savannah
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QC Sample Results
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-754395/14-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754609 Prep Batch: 754395
Indeno[1,2,3-cd]pyrene 6.54 6.437 mg/Kg 98 40 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Isophorone 6.54 4.908 mg/Kg 75 26 -130
Naphthalene 6.54 4.146 mg/Kg 63 25 -130
Nitrobenzene 6.54 4.695 mg/Kg 72 25 -130
N-Nitrosodi-n-propylamine 6.54 4.741 mg/Kg 73 24 -130
N-Nitrosodiphenylamine 6.54 5.036 mg/Kg 77 37 -130
Pentachlorophenol 13.1 11.23 mg/Kg 86 16 -135
Phenanthrene 6.54 5.084 mg/Kg 78 38 -130
Phenol 6.54 5.360 mg/Kg 82 27 -130
Pyrene 6.54 5.905 mg/Kg 90 40 -130
2,4,6-Tribromophenol (Surr)21 -132
Surrogate
99
LCS LCS
Qualifier Limits%Recovery
742-Fluorobiphenyl (Surr)25 -130
752-Fluorophenol (Surr)18 -130
70Nitrobenzene-d5 (Surr)19 -130
79Phenol-d5 (Surr)21 -130
92Terphenyl-d14 (Surr)31 -133
Method: 8015D - Gasoline Range Organics (GRO) (GC)
Client Sample ID: Method BlankLab Sample ID: MB 680-755508/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755508
RL MDL
Gasoline Range Organics [C6 - C10]ND 10.0 2.50 mg/Kg 12/16/22 16:13 100
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
a,a,a-Trifluorotoluene 77 70-131 12/16/22 16:13 100
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-755508/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755508
Gasoline Range Organics [C6 -
C10]
50.0 58.48 mg/Kg 117 64 -133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
a,a,a-Trifluorotoluene 70 -131
Surrogate
110
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-755508/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755508
Gasoline Range Organics [C6 -
C10]
50.0 60.12 mg/Kg 120 64 -133 3 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Eurofins Savannah
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QC Sample Results
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Method: 8015D - Gasoline Range Organics (GRO) (GC) (Continued)
a,a,a-Trifluorotoluene 70 -131
Surrogate
113
LCSD LCSD
Qualifier Limits%Recovery
Method: 8015D - Diesel Range Organics (DRO) (GC)
Client Sample ID: Method BlankLab Sample ID: MB 680-754292/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754473 Prep Batch: 754292
RL MDL
Diesel Range Organics [C10-C28]ND 7.82 2.54 mg/Kg 12/08/22 18:10 12/09/22 18:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
o-Terphenyl 62 15-139 12/09/22 18:24 1
MB MB
Surrogate
12/08/22 18:10
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-754292/4-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754473 Prep Batch: 754292
Diesel Range Organics
[C10-C28]
32.6 28.41 mg/Kg 87 26 -133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
o-Terphenyl 15 -139
Surrogate
85
LCS LCS
Qualifier Limits%Recovery
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: LB 680-755098/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755241 Prep Batch: 755098
RL MDL
Arsenic ND 0.0300 0.00860 mg/L 12/14/22 05:07 12/14/22 18:35 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.008900.0500 mg/L 12/14/22 05:07 12/14/22 18:35 1Barium
ND 0.0007800.00500 mg/L 12/14/22 05:07 12/14/22 18:35 1Cadmium
ND 0.02600.0500 mg/L 12/14/22 05:07 12/14/22 18:35 1Chromium
ND 0.003400.0250 mg/L 12/14/22 05:07 12/14/22 18:35 1Lead
ND 0.01200.0250 mg/L 12/14/22 05:07 12/14/22 18:35 1Selenium
ND 0.003900.0100 mg/L 12/14/22 05:07 12/14/22 18:35 1Silver
Client Sample ID: Method BlankLab Sample ID: LB2 680-755098/17-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755241 Prep Batch: 755098
RL MDL
Arsenic ND 0.0300 0.00860 mg/L 12/14/22 05:07 12/14/22 18:54 1
LB2 LB2
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.01370 J 0.008900.0500 mg/L 12/14/22 05:07 12/14/22 18:54 1Barium
ND 0.0007800.00500 mg/L 12/14/22 05:07 12/14/22 18:54 1Cadmium
ND 0.02600.0500 mg/L 12/14/22 05:07 12/14/22 18:54 1Chromium
ND 0.003400.0250 mg/L 12/14/22 05:07 12/14/22 18:54 1Lead
ND 0.01200.0250 mg/L 12/14/22 05:07 12/14/22 18:54 1Selenium
ND 0.003900.0100 mg/L 12/14/22 05:07 12/14/22 18:54 1Silver
Eurofins Savannah
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QC Sample Results
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: LB3 680-755098/18-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755241 Prep Batch: 755098
RL MDL
Arsenic ND 0.0300 0.00860 mg/L 12/14/22 05:07 12/14/22 18:58 1
LB3 LB3
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.01230 J 0.008900.0500 mg/L 12/14/22 05:07 12/14/22 18:58 1Barium
ND 0.0007800.00500 mg/L 12/14/22 05:07 12/14/22 18:58 1Cadmium
ND 0.02600.0500 mg/L 12/14/22 05:07 12/14/22 18:58 1Chromium
ND 0.003400.0250 mg/L 12/14/22 05:07 12/14/22 18:58 1Lead
ND 0.01200.0250 mg/L 12/14/22 05:07 12/14/22 18:58 1Selenium
ND 0.003900.0100 mg/L 12/14/22 05:07 12/14/22 18:58 1Silver
Client Sample ID: Method BlankLab Sample ID: MB 680-755098/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755241 Prep Batch: 755098
RL MDL
Arsenic ND 0.00300 0.000860 mg/L 12/14/22 05:07 12/14/22 18:27 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0008900.00500 mg/L 12/14/22 05:07 12/14/22 18:27 1Barium
ND 0.00007800.000500 mg/L 12/14/22 05:07 12/14/22 18:27 1Cadmium
ND 0.002600.00500 mg/L 12/14/22 05:07 12/14/22 18:27 1Chromium
ND 0.0003400.00250 mg/L 12/14/22 05:07 12/14/22 18:27 1Lead
ND 0.001200.00250 mg/L 12/14/22 05:07 12/14/22 18:27 1Selenium
ND 0.0003900.00100 mg/L 12/14/22 05:07 12/14/22 18:27 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-755098/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755241 Prep Batch: 755098
Arsenic 2.00 2.099 mg/L 105 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Barium 2.00 2.041 mg/L 102 80 -120
Cadmium 1.00 1.017 mg/L 102 80 -120
Chromium 2.00 2.054 mg/L 103 80 -120
Lead 10.1 10.56 mg/L 105 80 -120
Selenium 2.00 2.107 mg/L 105 80 -120
Silver 1.00 0.9475 mg/L 95 80 -120
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 680-754993/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755260 Prep Batch: 754993
RL MDL
Mercury ND 0.000200 0.000200 mg/L 12/14/22 07:33 12/14/22 17:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-754993/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755260 Prep Batch: 754993
Mercury 0.250 0.2459 mg/L 98 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Eurofins Savannah
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QC Sample Results
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Method: 7470A - Mercury (CVAA) (Continued)
Client Sample ID: Method BlankLab Sample ID: LB 680-754750/1-D
Matrix: Solid Prep Type: TCLP
Analysis Batch: 755260 Prep Batch: 754993
RL MDL
Mercury ND 0.0200 0.0200 mg/L 12/14/22 07:33 12/14/22 17:21 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Method BlankLab Sample ID: LB2 680-754750/13-D
Matrix: Solid Prep Type: TCLP
Analysis Batch: 755260 Prep Batch: 754993
RL MDL
Mercury ND 0.0200 0.0200 mg/L 12/14/22 07:33 12/14/22 18:02 1
LB2 LB2
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Method BlankLab Sample ID: LB3 680-754750/14-D
Matrix: Solid Prep Type: TCLP
Analysis Batch: 755260 Prep Batch: 754993
RL MDL
Mercury ND 0.0200 0.0200 mg/L 12/14/22 07:33 12/14/22 18:04 1
LB3 LB3
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Eurofins Savannah
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QC Association Summary
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
GC/MS VOA
Prep Batch: 753973
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035A680-226970-1 SS-C Total/NA
Analysis Batch: 754573
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260D 753973680-226970-1 SS-C Total/NA
Solid 8260DMB 680-754573/8 Method Blank Total/NA
Solid 8260DLCS 680-754573/5 Lab Control Sample Total/NA
Solid 8260DLCSD 680-754573/6 Lab Control Sample Dup Total/NA
GC/MS Semi VOA
Prep Batch: 754395
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3546680-226970-1 SS-C Total/NA
Solid 3546MB 680-754395/13-A Method Blank Total/NA
Solid 3546LCS 680-754395/14-A Lab Control Sample Total/NA
Analysis Batch: 754609
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270E 754395680-226970-1 SS-C Total/NA
Solid 8270E 754395MB 680-754395/13-A Method Blank Total/NA
Solid 8270E 754395LCS 680-754395/14-A Lab Control Sample Total/NA
GC VOA
Prep Batch: 753973
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035A680-226970-2 SS-B Total/NA
Analysis Batch: 755508
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015D 753973680-226970-2 SS-B Total/NA
Solid 8015DMB 680-755508/6 Method Blank Total/NA
Solid 8015DLCS 680-755508/4 Lab Control Sample Total/NA
Solid 8015DLCSD 680-755508/5 Lab Control Sample Dup Total/NA
GC Semi VOA
Prep Batch: 754292
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3546680-226970-2 SS-B Total/NA
Solid 3546MB 680-754292/3-A Method Blank Total/NA
Solid 3546LCS 680-754292/4-A Lab Control Sample Total/NA
Analysis Batch: 754473
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015D 754292680-226970-2 SS-B Total/NA
Solid 8015D 754292MB 680-754292/3-A Method Blank Total/NA
Solid 8015D 754292LCS 680-754292/4-A Lab Control Sample Total/NA
Eurofins Savannah
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QC Association Summary
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Metals
Leach Batch: 754750
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 1311680-226970-1 SS-C TCLP
Solid 1311LB 680-754750/1-D Method Blank TCLP
Solid 1311LB2 680-754750/13-D Method Blank TCLP
Solid 1311LB3 680-754750/14-D Method Blank TCLP
Prep Batch: 754993
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7470A 754750680-226970-1 SS-C TCLP
Solid 7470A 754750LB 680-754750/1-D Method Blank TCLP
Solid 7470A 754750LB2 680-754750/13-D Method Blank TCLP
Solid 7470A 754750LB3 680-754750/14-D Method Blank TCLP
Solid 7470AMB 680-754993/1-A Method Blank Total/NA
Solid 7470ALCS 680-754993/2-A Lab Control Sample Total/NA
Prep Batch: 755098
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3010A 754750680-226970-1 SS-C TCLP
Solid 3010ALB 680-755098/3-A Method Blank Total/NA
Solid 3010ALB2 680-755098/17-A Method Blank Total/NA
Solid 3010ALB3 680-755098/18-A Method Blank Total/NA
Solid 3010AMB 680-755098/1-A Method Blank Total/NA
Solid 3010ALCS 680-755098/2-A Lab Control Sample Total/NA
Analysis Batch: 755241
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6020B 755098680-226970-1 SS-C TCLP
Solid 6020B 755098LB 680-755098/3-A Method Blank Total/NA
Solid 6020B 755098LB2 680-755098/17-A Method Blank Total/NA
Solid 6020B 755098LB3 680-755098/18-A Method Blank Total/NA
Solid 6020B 755098MB 680-755098/1-A Method Blank Total/NA
Solid 6020B 755098LCS 680-755098/2-A Lab Control Sample Total/NA
Analysis Batch: 755260
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7470A 754993680-226970-1 SS-C TCLP
Solid 7470A 754993LB 680-754750/1-D Method Blank TCLP
Solid 7470A 754993LB2 680-754750/13-D Method Blank TCLP
Solid 7470A 754993LB3 680-754750/14-D Method Blank TCLP
Solid 7470A 754993MB 680-754993/1-A Method Blank Total/NA
Solid 7470A 754993LCS 680-754993/2-A Lab Control Sample Total/NA
General Chemistry
Analysis Batch: 754793
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture680-226970-1 SS-C Total/NA
Solid Moisture680-226970-2 SS-B Total/NA
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-226970-1
Project/Site: Yadkin County Transfer Station
Client Sample ID: SS-C Lab Sample ID: 680-226970-1
Matrix: SolidDate Collected: 12/05/22 09:15
Date Received: 12/06/22 10:30
Leach 1311 KF12/12/22 20:21 EET SAV754750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
TCLP 100.02 g 2000 mL
Prep 3010A 755098 12/14/22 05:07 RR EET SAVTCLP5 mL 250 mL
Analysis 6020B 1 755241 12/14/22 18:50 BWR EET SAVTCLP
ICPMSCInstrument ID:
Leach 1311 754750 12/12/22 20:21 KF EET SAVTCLP100.02 g 2000 mL
Prep 7470A 754993 12/14/22 07:33 JKL EET SAVTCLP0.50 mL 50 mL
Analysis 7470A 1 755260 12/14/22 17:49 JKL EET SAVTCLP
QuickTrace2Instrument ID:
Analysis Moisture 1 754793 12/13/22 08:03 WRB EET SAVTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: SS-C Lab Sample ID: 680-226970-1
Matrix: SolidDate Collected: 12/05/22 09:15
Percent Solids: 75.0Date Received: 12/06/22 10:30
Prep 5035A FES12/07/22 10:03 EET SAV753973
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.846 g 5 mL
Analysis 8260D 1 754573 12/11/22 21:39 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 754395 12/09/22 11:25 MEW EET SAVTotal/NA 15.61 g 1 mL
Analysis 8270E 1 754609 12/12/22 06:26 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Client Sample ID: SS-B Lab Sample ID: 680-226970-2
Matrix: SolidDate Collected: 12/05/22 09:45
Date Received: 12/06/22 10:30
Analysis Moisture WRB12/13/22 08:031 EET SAV754793
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: SS-B Lab Sample ID: 680-226970-2
Matrix: SolidDate Collected: 12/05/22 09:45
Percent Solids: 76.2Date Received: 12/06/22 10:30
Prep 5035A FES12/07/22 10:03 EET SAV753973
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.438 g 5 mL
Analysis 8015D 100 755508 12/16/22 16:35 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Prep 3546 754292 12/08/22 18:10 MJ EET SAVTotal/NA 30.24 g 1 mL
Analysis 8015D 1 754473 12/09/22 21:59 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
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Accreditation/Certification Summary
Client: S&ME, Inc.Job ID: 680-226970-1
Project/Site: Yadkin County Transfer Station
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 269 12-31-22
Eurofins Savannah
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Method Summary
Job ID: 680-226970-1Client: S&ME, Inc.
Project/Site: Yadkin County Transfer Station
Method Method Description LaboratoryProtocol
SW8468260DVolatile Organic Compounds by GC/MS EET SAV
SW8468270ESemivolatile Organic Compounds (GC/MS)EET SAV
SW8468015DGasoline Range Organics (GRO) (GC)EET SAV
SW8468015DDiesel Range Organics (DRO) (GC)EET SAV
SW8466020BMetals (ICP/MS)EET SAV
SW8467470AMercury (CVAA)EET SAV
EPAMoisturePercent Moisture EET SAV
SW8461311TCLP Extraction EET SAV
SW8463010APreparation, Total Metals EET SAV
SW8463546Microwave Extraction EET SAV
SW8465035AClosed System Purge & Trap EET SAV
SW8465035AClosed System Purge & Trap/Field Methanol EET SAV
SW8467470APreparation, Mercury EET SAV
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
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Login Sample Receipt Checklist
Client: S&ME, Inc.Job Number: 680-226970-1
Login Number: 226970
Question Answer Comment
Creator: Sims, Robert D
List Source: Eurofins Savannah
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Savannah
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