HomeMy WebLinkAboutWS-29767_48879_M_ESA_20230213 Phase II Environmental Site Assessment
Ramseur
1514 Main Street
Ramseur, North Carolina
EBI Project No. 1222000463
January 10, 2023
Prepared for:
American Postal Infrastructure Partners
1100 Jorie Blvd, Suite 207
Oak Brook, IL 60523
Prepared by:
Front overview picture of Subject Property [Click on Icon to Insert Picture]DELETE THIS TEXT BOX FROM DRAFT REPORT
ENVIROBUSINESS, INC. LOCATIONS | BALTIMORE, MD | BURLINGTON, MA | TEMPE AZ | IRVINE CA | SOUTHYORK
PA |QUINCY MA | RICHMOND VA
21 B Street
Burlington, MA 01803
Tel: (781) 273-2500
Fax: (781) 273-3311
www.ebiconsulting.com
January 10, 2023
Mr. Dylan Reilly
American Postal Infrastructure Partners
1100 Jorie Blvd, Suite 207
Oak Brook, IL 60523
Subject:Phase II Environmental Site Assessment
Ramseur
1514 Main Street Ramseur, North Carolina
EBI Project No. 1222000463
Dear Mr. Dylan Reilly:
In accordance with the Proposal and Standard Conditions for Engagement approved by yourself on December 7, 2022,
EBI Consulting (dba EBI Consulting, hereinafter “EBI”) is pleased to submit this Phase II Environmental Site
Assessment (ESA) for the above-referenced property (herein referred to as the Subject Property).
This Report is addressed to American Postal Infrastructure Partners. This Report is for the use and benefit of, and may
be relied upon by, American Postal Infrastructure Partners; initial and subsequent holders from time to time of any
debt and/or debt securities secured, directly or indirectly, any participation interest in such debt; any indenture
trustee, servicer, or other agent acting on behalf of such holders of such debt and/or debt securities; rating
agencies; and the institutional provider(s) from time to time of any liquidity facility or credit support for such
financings, and their respective successors and assigns.
The information contained in this report has received appropriate technical review and approval. The conclusions
represent professional judgments and are founded upon the findings of the investigations identified in the report
and the interpretation of such data based on our experience and expertise according to the existing standard of
care. No other warranty or limitation exists, either express or implied.
The conclusions of this Report are based on soil analytical data prepared by Pace Analytical Laboratory, soil screening
results obtained utilizing a field screening instrument, and field observations recorded by EBI personnel.
There are no intended or unintended third party beneficiaries to this Report, except as expressly stated herein.
EBI is an independent contractor, not an employee of either the issuer or the borrower, and its compensation was not
based on the findings or recommendations made in the Report or on the closing of any business transaction.
Thank you for the opportunity to prepare this Report, and assist you with this project. Please call us if you have any
questions or if we may be of further assistance.
Respectfully submitted,
EBI CONSULTING
Eric Routh
Author/Project Scientist
Stephanie Clorety, P.G.
Reviewer/Senior Project Manager
(443) 695-6135
Bruce Speidel, P.G.
Senior Program Director
(410) 552-1405
ENVIROBUSINESS, INC. LOCATIONS | BALTIMORE, MD | BURLINGTON, MA | TEMPE AZ | IRVINE CA | SOUTHYORK
PA |QUINCY MA | RICHMOND VA
21 B Street
Burlington, MA 01803
Tel: (781) 273-2500
Fax: (781) 273-3311
www.ebiconsulting.com
The Environmental Professionals listed above performed this Phase II ESA in general conformance with the ASTM
E1903-19 Standard Practice for Phase II ESAs. The listed individuals meet the qualifications for individuals
completing or overseeing all appropriate inquiries, and possess sufficient specific education, training, and
experience necessary to exercise professional judgment to develop opinions and conclusions regarding the
existence of environmental conditions on the property. Any work completed on this Phase II ESA by an individual
who is not considered an environmental professional was completed under the supervision or responsible charge
of the environmental professional.
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Phase II Environmental Site Assessment Ramseur
EBI Project #1222000463 1514 Main Street Ramseur, North Carolina
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Table of Contents
1.0 INTRODUCTION .........................................................................................................................1
1.1 Background.........................................................................................................................................................1
1.2 Statement of Objectives..................................................................................................................................1
1.3 Limitations and Assumptions..........................................................................................................................2
1.4 Special Terms and Conditions........................................................................................................................4
2.0 SUBJECT PROPERTY BACKGROUND..........................................................................................5
2.1 Subject Property Description and Features................................................................................................5
2.2 Physical Setting...................................................................................................................................................5
2.3 Site History and Land Use...............................................................................................................................6
2.4 Adjacent Property Land Use ..........................................................................................................................6
2.5 Summary of Previous Environmental Assessments...................................................................................6
3.0 RATIONALE AND WORK PERFORMED.......................................................................................7
3.1 Rationale..............................................................................................................................................................7
3.1.1 Conceptual Model....................................................................................................................................7
3.1.2 Rationale for Soil Boring Placement.....................................................................................................7
3.1.3 Chemical Testing Plan .............................................................................................................................8
3.1.4 Deviations from the Work Plan............................................................................................................8
3.2 Exploration, Sampling, and Test Screening Methods ................................................................................8
3.2.1 Ground Penetrating Radar Survey........................................................................................................8
3.2.2 Pre-Drilling Activities...............................................................................................................................8
3.2.3 Soil Borings ................................................................................................................................................9
3.2.4 Field Screening ..........................................................................................................................................9
3.2.5 Soil Sampling and Analysis....................................................................................................................10
3.2.9 Abandonment of Borings......................................................................................................................10
4.0 PRESENTATION OF EVALUATION AND RESULTS ....................................................................11
4.1 Soil Analysis Results .......................................................................................................................................11
5.0 FINDINGS & CONCLUSIONS ....................................................................................................13
6.0 RECOMMENDATIONS...............................................................................................................15
APPENDICES
APPENDIX A – FIGURES
FIGURE 1 – SITE LOCATION MAP
FIGURE 2 – TOPOGRAPHIC MAP
FIGURE 3 – BORING LOCATION MAP
APPENDIX B – BORING LOGS
APPENDIX C – LABORATORY ANALYTICAL RESULTS
APPENDIX D – PROFESSIONAL QUALIFICATIONS
APPENDIX E – GPR REPORT
Phase II Environmental Site Assessment Ramseur
EBI Project #1222000463 1514 Main Street Ramseur, North Carolina
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1.0 INTRODUCTION
In accordance with our Proposal and Standard Conditions for Engagement, EBI Consulting (EBI) is
pleased to submit our Phase II Environmental Site Assessment (ESA) Report (Report) on the property located
at 1514 Main Street, Ramseur, North Carolina (the Subject Property). Eric Routh of EBI Consulting
conducted the investigation at the Subject Property on December 21, 2022.
1.1 BACKGROUND
EBI was requested to conduct a Phase II ESA to evaluate the potential impact to the Subject Property
from the following item of environmental concern identified in EBI’s (November 17, 2022) Transaction
Screen report:
The Subject Property was identified in the underground storage tank (UST) database as Main Post
Office at 1514 Main Street. The UST listing identifies the subject property with a 1,000-gallon
heating oil tank installed on May 6, 1961. The tank is listed as constructed of single-walled steel. The
database does not identify a tank status or if the tank was permanently closed. EBI conducted a
search of available records online at the North Carolina Department of Environmental Quality
(NCDEQ) via their Public Records Search-UST Permits and Inspection Program, and did not identify
any records for the subject property. EBI submitted a request to the NCDEQ Winston Salem
Regional Office, to speak with the NCDEQ regarding the UST at the subject property. Mr. Michael
Phelps, Environmental Supervisor with the Division of Waste Management stated that the UST is a
non-registered tank and does not get inspected or require closure notification, so the NCDEQ does
not have any info on tank other than registration. Mr. Phelps checked their Registered UST database
and could not find any site on Main Street in Ramseur so he did not think the corrective action
branch has anything either, so the NCDEQ could not be sure if tank is still there or not. Based upon
the absence of documented removal and closure, the presence of the heating oil UST is considered
a Potential Environmental Concern (PEC) to the Subject Property.
1.2 STATEMENT OF OBJECTIVES
The primary objective of this Phase II ESA is to evaluate potential impact to the Subject Property from
the potential environmental concern (PEC) identified in the transaction screen prepared by EBI
(November 17, 2022) for the purpose of providing sufficient information regarding the nature and
potential extent of contamination to assist in making informed business decisions about the property;
and where applicable, providing the level of knowledge necessary to satisfy the innocent purchaser
defense under CERCLA. The investigation focused on the former heating oil UST.
In order to achieve the objectives of this investigation, EBI performed the following tasks:
Contacted the local utility locating service, North Carolina 811 (Ticket #A223491515) prior to
undertaking subsurface explorations on-site.
Contracted East Coast Geophysics, Inc. of Bensalem, Pennsylvania to conduct a ground penetrating
radar (GPR) survey of the accessible exterior areas of the Subject Property in an attempt to confirm
the presence or absence of potential remaining USTs and to clear each boring location before
undertaking subsurface explorations on-site.
Advanced three borings by Geoprobe direct push drill rig to depths of 14 to 19 feet below ground
surface (bgs).
Phase II Environmental Site Assessment Ramseur
EBI Project #1222000463 1514 Main Street Ramseur, North Carolina
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Collected four-foot soil samples continuously, field screened the vapor headspace of the soil
samples for total ionizable volatile organic compounds (VOCs) using a photoionization detector
(PID), and described the physical characteristics of the soil samples on boring logs.
Selected two soil samples per boring, prepared, and submitted the samples under chain-of-custody
documentation to a North Carolina-certified independent laboratory for analysis of total petroleum
hydrocarbons (TPH) - diesel range organics (DRO) via United States Environmental Protection
Agency (EPA) Method 8015B, VOCs via EPA Method 8260, and polynuclear aromatic hydrocarbons
(PAHs) via EPA Method 8270.
Prepared this summary of pertinent information obtained during this investigation including
accompanying illustrations and appendices, along with EBI’s findings and preliminary conclusions
regarding the presence or absence of contamination in soils beneath the Subject Property in the
areas investigated.
1.3 LIMITATIONS AND ASSUMPTIONS
This Report was prepared for the use of American Postal Infrastructure Partners. It was performed in
accordance with ASTM E1903-19, accepted practices of other consultants undertaking similar studies at
the same time and in the same locale under like circumstances. The conclusions provided by EBI are
based solely on the information obtained during the subsurface investigation. EBI renders no opinion as
to the presence of potential contamination in the areas not investigated. The observations in this Report
are valid on the date of the investigation. Any additional information that becomes available concerning
the Subject Property should be provided to EBI so that our conclusions may be revised and modified, if
necessary. This Report has been prepared in accordance with the proposal approved by American Postal
Infrastructure Partners and with the limitations and assumptions described below, all of which are integral
parts of this Report. No other warranty, expressed or implied, is made.
Limitations
1.The observations described in this Report were made under the conditions stated herein. The
conclusions presented are based solely upon the services described, and not on scientific tasks or
procedures beyond the scope of described services or the time and budgetary constraints imposed
by Client. The work described in this Report was carried out in accordance with terms and
conditions in our Authorization Letter and Agreement for Environmental Services regarding the
Site, which are incorporated herein by references.
2.In preparing this Report, EBI has relied on certain information provided by state and other
referenced parties, and on information contained in the files of federal, state and/or local agencies
available to EBI at the time of the assessment. Although there may have been some degree of
overlap in the information provided by these various sources, EBI did not attempt to independently
verify the accuracy or completeness of all information reviewed or received during the course of
these Environmental Services.
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EBI Project #1222000463 1514 Main Street Ramseur, North Carolina
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3.Observations were made of the Site and of structures on the Site as indicated within the Report.
Where access to portions of the Site or to structures on the Site was unavailable or limited, EBI
renders no opinion as to the presence of oil or hazardous materials (OHM) in that portion of the
Site or structure. In addition, EBI renders no opinion as to the presence of OHM or the presence
of indirect evidence relating to OHM where direct observation of the interior walls, floor, or ceiling
of a structure on a Site was obstructed by objects or coverings on or over these surfaces. No
representations concerning insulating material is expressed or implied.
4.EBI did not perform testing or analyses to determine the presence or concentration of asbestos,
radon, or lead at the Site unless specifically stated otherwise in the Report. Similarly, no
investigation of dust or air quality was conducted unless specifically stated otherwise in the Report.
5.The purpose of this Report is to assess the physical characteristics of the Site with respect to the
presence of OHM in the environment. No specific attempt was made to determine the compliance
of present or past owners or operators of the Site with federal, state, or local laws or regulations
(environmental or otherwise).
6.Except as noted in the Report, no quantitative laboratory testing was performed as part of the
assessment. Where such analyses have been conducted by an outside laboratory, EBI has relied
upon the data provided, and has not conducted an independent evaluation of the reliability of this
data.
7.Any qualitative or quantitative information regarding the Site, which was not available to EBI at the
time of this assessment may result in a modification of the representations made herein.
8.It is acknowledged that EBI judgments shall not be based on scientific or technical test or procedures
beyond the scope of the Services or beyond the time and budgetary constraints imposed by Client.
It is acknowledged further that EBI conclusions shall not rest on pure science but on such
considerations as economic feasibility and available alternatives. Client also acknowledges that,
because geologic and soil formations are inherently random, variable, and indeterminate in nature,
the Services and opinions provided under this Agreement with respect to such Services, are not
guaranteed to be a representation of actual conditions on the Site, which are also subject to change
with time as a result of natural or man-made processes, including water permeation. In performing
the Services, EBI shall use that degree of care and skill ordinarily exercised by environmental
consultants or engineers performing similar services in the same or similar locality. The standard of
care shall be determined solely at the time the Services are rendered and not according to standards
utilized at a later date. The Services shall be rendered without any other warranty, expressed or
implied, including, without limitation, the warranty of merchant ability and the warranty of fitness for
a particular purpose.
9.Client and EBI agree that to the fullest extent permitted by law, EBI shall not be liable to Client for
any special, indirect or consequential damages whatsoever, whether caused by EBI’S negligence,
errors, omissions, strict liability, breach of contract, breach of warranty or other cause of causes
whatsoever.
Assumptions
1.This Phase II ESA does not address the evaluation of business environmental risks in light of data
collected through the Phase II ESA process. Such evaluation is a function of site and transaction-
specific variables, and of the user’s objectives and risk tolerance. This practice contemplates that the
Phase II ESA process was planned and conducted with such variables in mind, and that the user will
evaluate legal, business and environmental risks in light of known data relating to the particular site
and transaction, and in consultation with legal and business advisors as well as the Phase II Assessor.
Phase II Environmental Site Assessment Ramseur
EBI Project #1222000463 1514 Main Street Ramseur, North Carolina
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2.The ASTM E1903-19 does not define the threshold levels at which target analytes pose a concern of
significance to the user. Users may apply this practice not only in light of applicable regulatory
criteria and relevant liability principles, but also to meet self-defined objectives.
3.The scope of work for this Phase II ESA is site-specific and context-specific. The assessment
process defined by ASTM E1903-19 is intended to generate sound, objective, and defensible
information sufficient to satisfy diverse user objectives.
4.No Phase II ESA can eliminate all uncertainty. Furthermore, any sample, either surface or
subsurface, taken for chemical testing may or may not be representative of a larger population.
Professional judgment and interpretation are inherent in the process, and even when exercised in
accordance with objective scientific principles, uncertainty is inevitable. Additional assessment
beyond that which was reasonably undertaken may reduce the uncertainty.
5.Even when Phase II ESA work is executed competently and in accordance with ASTM E1903-19, it
must be recognized that certain conditions present especially difficult target analyte detection
problems. Such conditions may include, but are not limited to, complex geological settings, unusual
or generally poorly understood behavior and fate characteristics of certain substances, complex,
discontinuous, random, or spotty distributions of existing target analytes, physical impediments to
investigation imposed by the location of utilities and other man-made objects, and the inherent
limitations of assessment technologies.
6.The Phase II ESA is intended to develop and present sound, scientifically valid data concerning actual
site conditions. It shall not be the role of the Phase II Assessor to provide legal or business advice.
1.4 SPECIAL TERMS AND CONDITIONS
This Phase II ESA (the report) has been prepared to assist American Postal Infrastructure Partners in its
underwriting of a proposed mortgage loan on the Subject Property. This report can be relied upon by
only the parties stated in the transmittal letter at the front of this report. EBI’s liability to a purchaser
wishing to use this report is limited to the cost of the report. Amendments to EBI’s limitations as stated
herein that may occur after issuance of the report are considered to be included in this report.
Payment for the report is made by, and EBI's contract and report extends to American Postal
Infrastructure Partners only, in accordance with our Standard Conditions for Engagement and,
Authorization Letter and Agreement for Environmental Services.
Phase II Environmental Site Assessment Ramseur
EBI Project #1222000463 1514 Main Street Ramseur, North Carolina
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2.0 SUBJECT PROPERTY BACKGROUND
2.1 SUBJECT PROPERTY DESCRIPTION AND FEATURES
Information regarding the Subject Property description, improvements, and operations is summarized
below:
PROPERTY DESCRIPTION, IMPROVEMENTS, AND OPERATIONS
Address 1514 Main Street, Ramseur, North Carolina
Location The Subject Property is located south of the intersection of Capel Street and
Main Street
Property Owner Levin Group, LLC
Number of Parcels 1
Total Land Area 0.3 acre
Number/Type of
Buildings
1/post office
Number of Stories 1
Date of Construction 1963
Basement No
Operations US Post Office
Site Characteristics The Subject Property is currently improved with one (1), post office building
and asphalt-paved parking lot.
2.2 PHYSICAL SETTING
Information regarding the physical settings at the Subject Property and immediate vicinity is summarized
below:
PHYSICAL SETTING DESCRIPTIONS
Regional Geology Information concerning the geology of the Subject Property was obtained from the
USGS National Water Summary, North Carolina region (1984). The Subject
Property is located within the Piedmont physiographic province, which is
characterized by gently rolling terrain and slow-flowing streams and is underlain by
hard crystalline and igneous rocks that are covered nearly everywhere by a clayey
or sandy regolith consisting of weathered parent rock material and alluvium.
Depth to Bedrock Bedrock was not encountered during the investigation.
Surficial Features Surface drainage on the Subject Property occurs over land to the adjoining wooded
land, primarily to the west. No indication of cross-lot runoff, swales, drainage
flows, or active rills or gullies were observed on the Subject Property.
Soil Stratigraphy
Encountered during
the Investigation
Soil stratigraphy encountered during the investigation consisted of approximately 8
to 9 feet of grayish/reddish/orangeish-brown clay with lesser amounts of sand,
underlain by brown/tan sand and clay and saprolite.
Estimated Direction of
Groundwater Flow
Local groundwater gradient is expected to follow surface topography; therefore,
groundwater flow near the Subject Property is expected to flow to the west.
Groundwater depths and flow gradients are best evaluated by a subsurface
investigation involving the installation of at least three groundwater-monitoring
wells, survey of well elevations, and precise measurements of hydraulic head.
Calculation of groundwater flow directions based on relative differences of
hydraulic head on the Subject Property was not included in this scope of work.
Depth to
Groundwater
(encountered during
the investigation)
Groundwater was not encountered during the investigation.
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EBI Project #1222000463 1514 Main Street Ramseur, North Carolina
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2.3 SITE HISTORY AND LAND USE
According to the transaction screen prepared by EBI (November 17, 2022), the site history and land use
is summarized in the following table:
Period Site History And Land Use
At least 1963 to
present
Existing building
2.4 ADJACENT PROPERTY LAND USE
Property use in the vicinity of the Subject Property is primarily characterized by commercial
development, as well as undeveloped, wooded land.
ADJOINING PROPERTIES
North The Subject Property is bound to the north by the Ramseur Public Library (1512 Main Street).
South The Subject Property is bound to the south by the Vera's Place (1518 Main Street).
East The Subject Property is bound to the east by Main Street, beyond which is Jordan Memorial United
Methodist Church (1511 Main Street).
West The Subject Property is bound to the north by undeveloped.
2.5 SUMMARY OF PREVIOUS ENVIRONMENTAL ASSESSMENTS
EBI was requested to conduct a Phase II ESA to evaluate the potential impact to the Subject Property
from the former UST based on the following recognized environmental concerns identified in EBI’s
(November 17, 2022) transaction screen Phase I ESA report:
The Subject Property was identified in the UST database as Main Post Office at 1514 Main Street.
The UST listing identifies the subject property with a 1,000-gallon heating oil tank installed on May 6,
1961. The tank is listed as constructed of single-walled steel. The database does not identify a tank
status or if the tank was permanently closed. EBI conducted a search of available records online at
the NCDEQ via their Public Records Search-UST Permits and Inspection Program, and did not
identify any records for the subject property. EBI submitted a request to the NCDEQ Winston
Salem Regional Office, to speak with the NCDEQ regarding the UST at the subject property. Mr.
Michael Phelps, Environmental Supervisor with the Division of Waste Management stated that the
UST is a non-registered tank and does not get inspected or require closure notification, so the
NCDEQ does not have any info on tank other than registration. Mr. Phelps checked their
Registered UST database and could not find any site on Main Street in Ramseur so he did not think
the corrective action branch has anything either, so the NCDEQ could not be sure if tank is still
there or not. Based upon the absence of documented removal and closure, the presence of the
heating oil UST is considered a PEC to the Subject Property.
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EBI Project #1222000463 1514 Main Street Ramseur, North Carolina
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3.0 RATIONALE AND WORK PERFORMED
3.1 RATIONALE
3.1.1 Conceptual Model
The Conceptual Model is a representation of hypothesized current site conditions, which describes the
physical setting characteristics of a site and the likely distribution of target contaminants (in soil, air,
ground water, surface water and/or sediments) that might have resulted from a known or likely release
and the risk they pose to human and/or ecological receptors. This Conceptual Model takes into
consideration the potential distributions of contaminants with respect to the properties, behaviors and
fate and transport characteristics of the contaminant in a setting such as that being assessed. The
sampling plan was designed to provide for the collection of potentially contaminated environmental
media, if they occur, at locations and depths where the highest concentrations are likely to occur.
Site Environmental Concerns Site Physical Characteristics Onsite Environmental
Receptors
RECs COC’s Primary
Release
Media
Fate &
Transport
Potential
Exposure
Route(s)
Potential
Human
Exposure
UST Volatile organic
compounds
(VOCs)
Total petroleum
hydrocarbons
(TPH) – Diesel
range organics
(DRO)
Polynuclear
aromatic
hydrocarbons
(PAHs)
Soil Soil
Soil Vapor
Groundwater
Indoor Air
Ingestion
Inhalation
Dermal (direct
Contact)
Tenants
Site workers
Construction
workers
COC = contaminants of concern
Assumptions:
1.Assumes the Subject Property retains existing use
2.Construction Worker exposure is limited due to short exposure duration
3.1.2 Rationale for Soil Boring Placement
The rationale for the placement of the soil borings was based on the 1) the Likely Release Areas that
target analytes were first introduced into environmental media as a result of a release; and 2) the likely
vertical and horizontal migration of the release.
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3.1.3 Chemical Testing Plan
The chemical testing plan was designed to detect the target analytes that are present in, or have been
released or potentially have been released to, environmental media at the site, and which are of interest
in the context of the particular Phase II ESA and its objectives, the presence of which will be sought and
concentrations of which will be quantified through chemical testing.
3.1.4 Deviations from the Work Plan
There were no deviations to the work plan.
3.2 EXPLORATION, SAMPLING, AND TEST SCREENING METHODS
3.2.1 Ground Penetrating Radar Survey
EBI contracted East Coast Geophysics, Inc. of Bensalem, Pennsylvania to conduct a ground penetrating
radar (GPR) survey of the accessible exterior areas of the Subject Property in an attempt to confirm the
presence or absence of potential remaining USTs. The GPR survey was conducted at the Subject
Property on December 21, 2022. GPR equipment was used in an attempt to locate potential USTs as
well as to define the presence, size, and depth of any potential USTs and/or former UST locations. GPR
is a geophysical technique, which uses electromagnetic waves for shallow subsurface reconnaissance and
exploration. An electromagnetic impulse in the form of ultra high-frequency radio waves is emitted into
the ground by the transmitting antenna, and the resulting reflection of transfer of waves from
contamination plumes, boundary layers, or buried objects is detected by a receiving antenna. The
presence of buried objects or significant changes in conductivity of the layers will cause the
electromagnetic wave to be reflected. These images provide direct information concerning subsurface
conditions. EBI notes that due to surface conditions and subsurface content, the GPR signal penetration
was estimated at 1 to 3 feet in the majority of the survey area. This penetration was reduced in areas of
concrete cover. In addition, due to the dielectric properties of the subsurface, plastic polymer and
fiberglass utilities may not have been detected. All field services were conducted in compliance with the
general industry standard practices.
The results of the GPR survey did not identify anomalies indicative of a UST located beneath the
surveyed areas of the Subject Property. GPR transects imaged what appeared to be a former
excavation located on the northwest corner of the Subject Property building. The potential former
excavation measures approximately 13 feet by 6 feet. The feature is located on the northwest corner of
the Subject Property building. The feature is located below a cutout concrete pad and an AST. A copy
of the GPR report is presented in Appendix E.
3.2.2 Pre-Drilling Activities
Cardno Inc. requested North Carolina 811 to mark-out the location of Subject Property utilities on
December 15, 2022. Clearance for drilling at the Subject Property was granted for after 7:00 AM on
December 20, 2022. EBI also contracted with a private utility locating company, East Coast Geophysics
Inc. to clear each boring location before undertaking subsurface explorations on-site.
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Personal health and safety precautions were followed in accordance with applicable federal and state law
or local equivalents and any requirements imposed by the owner, occupant, or field personnel. EBI
prepared a site-specific health and safety plan (HASP) and conducted a health and safety meeting with
the onsite personnel prior to the drilling activities. No additional pre-drilling activities were performed
as part of this investigation.
3.2.3 Soil Borings
A total of three borings were advanced at the Subject Property. All of the soil borings were advanced
using a direct push drill rig Cardno Inc. of Richmond, Virginia. Four-foot soil samples were collected
continuously during the advancement of the borings. EBI recorded soil sampling information and the
physical characteristics of each soil sample onto boring logs presented in Appendix B.
TABLE 3.2.3
SUMMARY OF SOIL BORING DETAILS
Boring
ID#
Location Termination
Depth/Reason
(feet bgs)
Depth to
Groundwater
(feet)
Sample ID #/
Depths
Target Analytes/
EPA Method
B1 Directly west of the
GPR identified
former excavation
17
(equipment refusal)
Not
encountered
Soil B1(5-7)
Soil B1(12-14)
VOCs/8260
PAHs/8270
TPH-DRO/8015
B2 Directly southwest
of the GPR
identified former
excavation
19
(equipment refusal)
Not
encountered
Soil B2(6-8)
Soil B2(17-19)
VOCs/8260
PAHs/8270
TPH-DRO/8015
B3 Center of GPR
identified former
excavation
14 (equipment
refusal)
Not
Encountered
Soil B3(6-8)
Soil B3(12-14)
VOCs/8260
PAHs/8270
TPH-DRO/8015
Notes: TPH - Total petroleum hydrocarbons via EPA Method 8015
VOCs -Volatile organic compounds via EPA Method 8260
PAH - Polynuclear aromatic hydrocarbons via EPA Method 8270.
B – Boring
(#-#) – Depth below grade sample collected.
Boring locations are illustrated on Figure 3, Boring Location Map.
3.2.4 Field Screening
The vapor headspace of each soil sample was field-screened using a PID. The PID provides a reading of
total ionizable VOCs. The PID was calibrated with an isobutylene standard, to measure total VOCs as
isobutylene equivalents. The PID has a practical sensitivity of approximately one part per million by
volume (ppmV). PID readings should not be considered as exact measurements, but as relative readings
of VOCs between locations. The soil samples were placed in a ziplock bag approximately three-
quarters full with the soil to be analyzed, which was sealed for approximately 10 minutes in a warm
(>60˚ F) location for equilibration. The headspace analysis was conducted by inserting the probe of the
PID through an opening in the zip-lock bag and into the space above the soil sample.
Petroleum odors were observed in soil from borings B1 and B3. PID readings ranged from 0.0 to 278.3
parts per million (ppm). The PID results are noted in the Boring Logs provided in Appendix B.
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EBI Project #1222000463 1514 Main Street Ramseur, North Carolina
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3.2.5 Soil Sampling and Analysis
Selected “grab” soil samples were collected in laboratory-provided sample containers. Each sample was
labeled/logged onto a chain-of-custody form, and placed in a cooler with ice for preservation in
accordance with current Federal EPA SW-846 (3rd ed.). The samples were submitted to an
independent qualified laboratory (Pace Analytical) for analyses. The samples were analyzed for the target
analytes noted in Table 3.2.3.
Samples submitted for VOC analysis were also preserved with methanol in accordance with EPA
Method 8260.
In order to ensure that no cross-contamination between samples occurred, all non-dedicated sampling
equipment was decontaminated after the collection of each sample. Sampling equipment was scrubbed
with a brush to remove loose material and then washed thoroughly with a laboratory grade detergent
and water to remove all particulate matter and surface film. After washing, each piece and brush was
rinsed with clean distilled water. Dedicated sampling equipment such as sampling liners and nitrile gloves
were properly disposed of after the handling of each sample was complete. Samples were then collected
using clean disposable gloves and laboratory-provided glassware appropriate for the specified analysis.
3.2.9 Abandonment of Borings
Upon completion of the soil sampling activities, each soil boring was filled with the soil cuttings
generated during the sampling activities. The remaining void in each borehole was filled with granular
bentonite. The top two to four inches were backfilled with asphalt and compacted.
Phase II Environmental Site Assessment Ramseur
EBI Project #1222000463 1514 Main Street Ramseur, North Carolina
11
4.0 PRESENTATION OF EVALUATION AND RESULTS
4.1 SOIL ANALYSIS RESULTS
The samples were analyzed for the target analytes noted in Table 3.2.3. The following table presents only
the contaminants identified above the laboratory method detection limits:
Table 4.1 Soil Results
Results flagged as "Exceed" if any of the selected criteria exceeded (most stringent).Legend:Hit Exceed
Client Sample ID:B1 (5-7)B1 (12-14)B2 (6-8)
Date Sampled:12/21/2022 12/21/2022 12/21/2022
Matrix:
NCDEQ MSCCs - Soil to Groundwater
NCDEQ MSCCs - Residential Soil
NCDEQ MSCCs - Industrial Soil Soil Soil Soil
TPH-DRO
TPH-DRO mg/kg 31 469 7000 610 192 9.9
VOCs
N-Butylbenzene mg/kg 2.4 782 11600 1.41 0.0861 ND
Sec-Butylbenzene mg/kg 2.2 1560 23300 1.18 0.122 ND
Tert-Butylbenzene mg/kg 1.7 1560 23300 0.575 ND ND
Ethylbenzene mg/kg 8 60.3 297 0.3 0.0127 ND
Isopropylbenzene mg/kg 1.3 1560 23300 0.47 0.0307 ND
Naphthalene mg/kg 0.2 5.5 27 8.94 0.362 ND
N-Propylbenzene mg/kg 1.4 1560 23300 0.732 0.0627 ND
1,2,4-Trimethylbenzene mg/kg 6.6 156 2330 ND 0.0609 ND
1,3,5-Trimethylbenzene mg/kg 6.6 156 2330 ND ND ND
PAHs
Anthracene mg/kg 640 4600 7000 0.163 0.00845 ND
Acenaphthene mg/kg 8.3 930 14000 1.59 0.133 ND
Acenaphthylene mg/kg 20 930 14000 ND 0.0337 ND
Benzo(A)Anthracene mg/kg 0.17 6.6 32 1.5 ND ND
Benzo(A)Pyrene mg/kg 0.058 0.66 3.2 1.26 ND ND
Benzo(B)Fluoranthene mg/kg 0.6 6.6 32 1.52 ND ND
Benzo(G,H,I)Perylene mg/kg 7600 469 7000 0.752 ND ND
Benzo(K)Fluoranthene mg/kg 5.8 66 327 0.556 ND ND
Chrysene mg/kg 18 663 3270 1.17 ND ND
Dibenz(A,H)Anthracene mg/kg 0.19 0.66 3.27 0.191 ND ND
Fluoranthene mg/kg 330 625 9340 1.29 0.00774 ND
Fluorene mg/kg 55 625 9340 2.01 0.173 ND
Indeno(1,2,3-Cd)Pyrene mg/kg 1.9 6.63 32.7 0.919 ND ND
Naphthalene mg/kg 0.2 5.5 27 5.32 0.175 ND
Phenanthrene mg/kg 64 469 7000 2.74 0.357 ND
Pyrene mg/kg 210 469 7000 1.14 0.0181 ND
1-Methylnaphthalene mg/kg 0,054 22.8 112 11.2 0.969 ND
2-Methylnaphthalene mg/kg 1.5 62.5 934 21 1.3 ND
Client Sample ID:B2 (17-19)B3 (6-8)B3 (12-14)
Date Sampled:12/21/2022 12/21/2022 12/21/2022
Matrix:
NCDEQ MSCCs - Soil to Groundwater
NCDEQ MSCCs - Residential
Soil
NCDEQ MSCCs - Industrial Soil Soil Soil Soil
TPH-DRO
TPH-DRO mg/kg 31 469 7000 31.9 987 734
VOCs
N-Butylbenzene mg/kg 2.4 782 11600 ND 1.28 1.53
Sec-Butylbenzene mg/kg 2.2 1560 23300 ND 1.15 1.27
Tert-Butylbenzene mg/kg 1.7 1560 23300 ND ND ND
Ethylbenzene mg/kg 8 60.3 297 ND 0.39 0.825
Isopropylbenzene mg/kg 1.3 1560 23300 ND 0.743 0.831
Naphthalene mg/kg 0.2 5.5 27 0.0196 3.98 1.88
N-Propylbenzene mg/kg 1.4 1560 23300 ND 1.11 1.24
1,2,4-Trimethylbenzene mg/kg 6.6 156 2330 0.0169 ND ND
1,3,5-Trimethylbenzene mg/kg 6.6 156 2330 0.00647 ND ND
Phase II Environmental Site Assessment Ramseur
EBI Project #1222000463 1514 Main Street Ramseur, North Carolina
12
Table 4.1 Soil Results
Results flagged as "Exceed" if any of the selected criteria exceeded (most stringent).Legend:Hit Exceed
Client Sample ID:B2 (17-19)B3 (6-8)B3 (12-14)
Date Sampled:12/21/2022 12/21/2022 12/21/2022
Matrix:
NCDEQ MSCCs
- Soil to Groundwater
NCDEQ
MSCCs - Residential Soil
NCDEQ
MSCCs - Industrial Soil
Soil Soil Soil
PAHs
Anthracene mg/kg 640 4600 7000 ND 0.0648 0.0672
Acenaphthene mg/kg 8.3 930 14000 0.0169 0.746 0.572
Acenaphthylene mg/kg 20 930 14000 ND ND ND
Benzo(A)Anthracene mg/kg 0.17 6.6 32 ND ND ND
Benzo(A)Pyrene mg/kg 0.058 0.66 3.2 ND ND ND
Benzo(B)Fluoranthene mg/kg 0.6 6.6 32 ND ND ND
Benzo(G,H,I)Perylene mg/kg 7600 469 7000 ND ND ND
Benzo(K)Fluoranthene mg/kg 5.8 66 327 ND ND ND
Chrysene mg/kg 18 663 3270 ND ND ND
Dibenz(A,H)Anthracene mg/kg 0.19 0.66 3.27 ND ND ND
Fluoranthene mg/kg 330 625 9340 ND 0.0501 0.0414
Fluorene mg/kg 55 625 9340 0.0411 1 0.793
Indeno(1,2,3-Cd)Pyrene mg/kg 1.9 6.63 32.7 ND ND ND
Naphthalene mg/kg 0.2 5.5 27 ND 1.83 0.502
Phenanthrene mg/kg 64 469 7000 0.13 1.82 1.62
Pyrene mg/kg 210 469 7000 ND 0.186 0.157
1-Methylnaphthalene mg/kg 0,054 22.8 112 0.133 4.72 3.1
2-Methylnaphthalene mg/kg 1.5 62.5 934 0.213 7.89 2.63
Notes:All results are shown in milligrams per kilogram (mg/kg)
ND = Non-detected above laboratory detection limits
The analytical results revealed that concentrations of TPH-DRO, VOCs, and PAHs were detected above
laboratory detection limits in the soil samples analyzed. None of the concentrations identified exceeded
the NCDEQ Maximum Soil Contaminant Concentrations (MSCCs) for Commercial/Industrial direct
contact. The concentrations of TPH-DRO, naphthalene and several PAHs exceeded the NCDEQ
MSCCs for Soil to Groundwater and Residential direct contact in the soil samples collected.
Laboratory soil analytical results and complete laboratory data sheets and chain-of-custody
documentation are presented in Appendix C.
Phase II Environmental Site Assessment Ramseur
EBI Project #1222000463 1514 Main Street Ramseur, North Carolina
13
5.0 FINDINGS & CONCLUSIONS
We have performed a Phase II ESA at the property at 1514 Main Street, North Carolina, in general
conformance with the scope and limitations of ASTM E1903-19 and for the following objectives:
The primary objective of this Phase II ESA is to evaluate potential impact to the Subject Property
from the PEC identified in the transaction screen prepared by EBI (November 17, 2022) for the
purpose of providing sufficient information regarding the nature and potential extent of
contamination to assist in making informed business decisions about the property; and where
applicable, providing the level of knowledge necessary to satisfy the innocent purchaser defense
under CERCLA. The investigation focused on the former heating oil UST.
Findings
The results of EBI's Phase II ESA revealed:
On December 21, 2022, EBI conducted a GPR survey was completed to determine if any former
UST exist at the Subject Property. The results of the GPR survey did not identify anomalies
indicative of a UST located beneath the surveyed areas of the Subject Property. GPR transects
imaged what appeared to be a former excavation located on the northwest corner of the Subject
Property building. The potential former excavation measures approximately 13 feet by 6 feet. The
feature is located on the northwest corner of the Subject Property building. The feature is located
below a cutout concrete pad and an AST.
On December 21, 2022, EBI conducted a Phase II ESA to assess subsurface conditions at the Subject
Property. A total of three soil borings were advanced at the Subject Property. Groundwater was
not encountered during the investigation. All of the soil borings were advanced using a direct push
drill rig. The samples were submitted to a North Carolina-certified laboratory, Pace Analytical, for
analysis of VOCs via EPA Method 8260, PAHs via EPA Method 8270, and TPH-DRO via EPA
Method 8015B.
The analytical results revealed that concentrations of TPH-DRO, VOCs, and PAHs were detected
above laboratory detection limits in the soil samples analyzed. Insert description here based on
residential/industrial standards
Conclusions
The results of the GPR survey did not identify anomalies indicative of a UST located beneath the
surveyed areas of the Subject Property. GPR transects imaged what appeared to be a former
excavation located on the northwest corner of the Subject Property building. The potential former
excavation measures approximately 13 feet by 6 feet.
The analytical results revealed that concentrations of TPH-DRO, VOCs, and PAHs were detected
above laboratory detection limits in the soil samples analyzed. None of the concentrations
identified exceeded the NCDEQ MSCCs for Commercial/Industrial direct contact. The
concentrations of TPH-DRO, naphthalene and several PAHs exceeded the NCDEQ MSCCs for Soil
to Groundwater and Residential direct contact in the soil samples collected.
EBI notes that according to the NCDEQ Division of Waste Management (DWM), if contamination is
discovered or evidence of a release is identified, a reporting condition to the NCDEQ DWM exists.
Phase II Environmental Site Assessment Ramseur
EBI Project #1222000463 1514 Main Street Ramseur, North Carolina
14
6.0 RECOMMENDATIONS
Based on the findings and conclusions of this Phase II ESA, EBI recommends the following:
EBI notes that due to the detection of petroleum constituents in the soil, a reporting requirement to
the NCDEQ appears to exist. EBI recommends providing the results to the owner/operator. The
owner/operator should discuss the NCDEQ reporting requirements with their legal counsel. If
reported to the NCDEQ, upon completion of their review of this report, additional investigation
may be required to further evaluate the petroleum impact.
APPENDIX A
FIGURES
FIGURE 1 – SITE LOCATION MAP
Not to scale
To ROTATE orientation of North
Arrow: Click on the Arrow, then
grab and rotate the green dot; or
Double-Click on the Arrow, then
select the Size Tab, then adjust
the rotation by degrees.
DELETE THIS TEXT BOX
FROM DRAFT REPORT
Subject Property
FIGURE 2 – TOPOGRAPHIC MAP
Not to scale
Subject Property
FIGURE 3 – BORING LOCATION MAP
Boring Location
Not to scale
GPR identified potential
former excavation
B3
B2
B1
APPENDIX B
BORING LOGS
SOIL BORING LOG - FIELD READINGS
EBI Project No. 1222000463
Project Name: Ramseur
BORING METHOD: Geoprobe DATE: December 21, 2022
Sample #Depth (Ft)Moisture (Saturated
– Moist - Dry)
PID Reading
(ppm)
Soil Description/Notes
B1 0-3 Moist 0.0 Reddish brown clay, trace sand
B1 3-7 Moist 3-4’: 3.1
4-5’: 4.5
5-7’: 37.3
Grayish brown clay, trace sand, petroleum odor
B1 7-9 Moist 7-8’: 15.2 Reddish brown clay, trace sand, petroleum odor
B1 9-12 Moist 8-10’: 35.2
10-12’: 76.7
Tan sandy clay, petroleum odor
B1 12-17 Moist 12-14’: 96.2
14-17’: 55.3
Tan fine sand, silt, saprolite, petroleum odor
Bottom of Boring at 17’ (equipment refusal), no groundwater encountered
B2 0-3 Moist 0.0 Orangish gray/tan clay
B2 3-9 Moist 0.0 Red, gray, brown clay
B2 9-13 Moist 0.0 Reddish tan fine sand, clay
B2 13-19 Moist 0.0 Tan fine sand, clay, sapprolite
Bottom of Boring at 19’ (equipment refusal), no groundwater encountered
B3 0-6 Moist 0-4’: 0.0
4-6’: 55.2
Gray sand, silt, gravel fill
B3 6-13 Moist 6-8’: 278.3
8-10’: 53.1
10-12’: 67.3
12-13’: 79.1
Reddish/orangish brown clay, sand, silt
B3 13-14 Moist 73.2 Brown/tan clay, sand, saprolite
Bottom of Boring at 10’ (Termination depth), no groundwater encountered
APPENDIX C
LABORATORY ANALYTICAL RESULTS
ANALYTICAL REPORT
January 05, 2023
EBI Consulting
Sample Delivery Group:L1570312
Samples Received:12/22/2022
Project Number:EBICONPAZ-1222000463
Description:Ramseur NC
Report To:Eric Routh
21 B Street
Burlington, MA 01803
Entire Report Reviewed By:
January 05, 2023
[Preliminary Report]
Daphne Richards
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
B1 (12-14) L1570312-01 5
B1 (5-7) L1570312-02 7
B2 (6-8) L1570312-03 10
B2 (17-19) L1570312-04 12
B3 (6-8) L1570312-05 14
B3 (12-14) L1570312-06 17
Qc: Quality Control Summary 19
Total Solids by Method 2540 G-2011 19
Volatile Organic Compounds (GC/MS) by Method 8260B 20
Semi-Volatile Organic Compounds (GC) by Method 8015 28
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM 29
Gl: Glossary of Terms 32
Al: Accreditations & Locations 33
Sc: Sample Chain of Custody 34
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5Sr
6Qc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
B1 (12-14) L1570312-01 Solid 12/21/22 10:25 12/22/22 10:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1980780 1 12/29/22 09:50 12/29/22 10:13 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG1982417 4 12/21/22 10:25 01/03/23 14:41 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG1980058 20 12/29/22 05:04 12/29/22 14:49 JAS Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG1980069 1 12/28/22 08:52 12/28/22 17:36 DSH Mt. Juliet, TN
Collected by Collected date/time Received date/time
B1 (5-7) L1570312-02 Solid 12/21/22 10:25 12/22/22 10:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1980780 1 12/29/22 09:50 12/29/22 10:13 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG1981849 80 12/21/22 10:25 12/31/22 19:47 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG1980058 10 12/29/22 05:04 12/29/22 13:57 JAS Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG1980069 1 12/28/22 08:52 12/28/22 16:43 ADF Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG1980069 10 12/28/22 08:52 12/29/22 22:34 ADF Mt. Juliet, TN
Collected by Collected date/time Received date/time
B2 (6-8) L1570312-03 Solid 12/21/22 11:10 12/22/22 10:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1980780 1 12/29/22 09:50 12/29/22 10:13 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG1981849 1 12/21/22 11:10 12/31/22 18:21 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG1980058 1 12/29/22 05:04 12/29/22 16:20 KAP Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG1980069 1 12/28/22 08:52 12/28/22 16:25 DSH Mt. Juliet, TN
Collected by Collected date/time Received date/time
B2 (17-19) L1570312-04 Solid 12/21/22 11:10 12/22/22 10:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1980780 1 12/29/22 09:50 12/29/22 10:13 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG1981849 1 12/21/22 11:10 12/31/22 18:43 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG1980058 1 12/29/22 05:04 12/29/22 11:47 JAS Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG1980069 1 12/28/22 08:52 12/28/22 13:10 DSH Mt. Juliet, TN
Collected by Collected date/time Received date/time
B3 (6-8) L1570312-05 Solid 12/21/22 12:20 12/22/22 10:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1980780 1 12/29/22 09:50 12/29/22 10:13 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG1981849 80 12/21/22 12:20 12/31/22 20:09 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG1980058 10 12/29/22 05:04 12/29/22 14:23 JAS Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG1980069 1 12/28/22 08:52 12/28/22 15:50 ADF Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG1980069 5 12/28/22 08:52 12/29/22 21:23 JRM Mt. Juliet, TN
Collected by Collected date/time Received date/time
B3 (12-14) L1570312-06 Solid 12/21/22 12:20 12/22/22 10:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1980780 1 12/29/22 09:50 12/29/22 10:13 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG1981849 80 12/21/22 12:20 12/31/22 20:30 JHH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015 WG1980058 10 12/29/22 05:04 12/29/22 14:36 JAS Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM WG1980069 1 12/28/22 08:52 12/28/22 15:32 DSH Mt. Juliet, TN
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Daphne Richards
Project Manager
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SAMPLE RESULTS - 01
L1570312
B1 (12-14)
Collected date/time: 12/21/22 10:25
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 82.5 1 12/29/2022 10:13 WG1980780
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.200 4 01/03/2023 14:41 WG1982417
Acrylonitrile ND 0.0500 4 01/03/2023 14:41 WG1982417
Benzene ND 0.00400 4 01/03/2023 14:41 WG1982417
Bromobenzene ND 0.0500 4 01/03/2023 14:41 WG1982417
Bromodichloromethane ND 0.0100 4 01/03/2023 14:41 WG1982417
Bromoform ND 0.100 4 01/03/2023 14:41 WG1982417
Bromomethane ND J4 0.0500 4 01/03/2023 14:41 WG1982417
n-Butylbenzene 0.0861 0.0500 4 01/03/2023 14:41 WG1982417
sec-Butylbenzene 0.122 0.0500 4 01/03/2023 14:41 WG1982417
tert-Butylbenzene ND 0.0200 4 01/03/2023 14:41 WG1982417
Carbon tetrachloride ND 0.0200 4 01/03/2023 14:41 WG1982417
Chlorobenzene ND 0.0100 4 01/03/2023 14:41 WG1982417
Chlorodibromomethane ND 0.0100 4 01/03/2023 14:41 WG1982417
Chloroethane ND 0.0200 4 01/03/2023 14:41 WG1982417
Chloroform ND 0.0100 4 01/03/2023 14:41 WG1982417
Chloromethane ND 0.0500 4 01/03/2023 14:41 WG1982417
2-Chlorotoluene ND 0.0100 4 01/03/2023 14:41 WG1982417
4-Chlorotoluene ND 0.0200 4 01/03/2023 14:41 WG1982417
1,2-Dibromo-3-Chloropropane ND 0.100 4 01/03/2023 14:41 WG1982417
1,2-Dibromoethane ND 0.0100 4 01/03/2023 14:41 WG1982417
Dibromomethane ND 0.0200 4 01/03/2023 14:41 WG1982417
1,2-Dichlorobenzene ND 0.0200 4 01/03/2023 14:41 WG1982417
1,3-Dichlorobenzene ND 0.0200 4 01/03/2023 14:41 WG1982417
1,4-Dichlorobenzene ND 0.0200 4 01/03/2023 14:41 WG1982417
Dichlorodifluoromethane ND 0.0100 4 01/03/2023 14:41 WG1982417
1,1-Dichloroethane ND 0.0100 4 01/03/2023 14:41 WG1982417
1,2-Dichloroethane ND 0.0100 4 01/03/2023 14:41 WG1982417
1,1-Dichloroethene ND 0.0100 4 01/03/2023 14:41 WG1982417
cis-1,2-Dichloroethene ND 0.0100 4 01/03/2023 14:41 WG1982417
trans-1,2-Dichloroethene ND 0.0200 4 01/03/2023 14:41 WG1982417
1,2-Dichloropropane ND 0.0200 4 01/03/2023 14:41 WG1982417
1,1-Dichloropropene ND 0.0100 4 01/03/2023 14:41 WG1982417
1,3-Dichloropropane ND 0.0200 4 01/03/2023 14:41 WG1982417
cis-1,3-Dichloropropene ND 0.0100 4 01/03/2023 14:41 WG1982417
trans-1,3-Dichloropropene ND 0.0200 4 01/03/2023 14:41 WG1982417
2,2-Dichloropropane ND 0.0100 4 01/03/2023 14:41 WG1982417
Di-isopropyl ether ND 0.00400 4 01/03/2023 14:41 WG1982417
Ethylbenzene 0.0127 0.0100 4 01/03/2023 14:41 WG1982417
Hexachloro-1,3-butadiene ND 0.100 4 01/03/2023 14:41 WG1982417
Isopropylbenzene 0.0307 0.0100 4 01/03/2023 14:41 WG1982417
p-Isopropyltoluene ND 0.0200 4 01/03/2023 14:41 WG1982417
2-Butanone (MEK)ND 0.400 4 01/03/2023 14:41 WG1982417
Methylene Chloride ND 0.100 4 01/03/2023 14:41 WG1982417
4-Methyl-2-pentanone (MIBK)ND 0.100 4 01/03/2023 14:41 WG1982417
Methyl tert-butyl ether ND 0.00400 4 01/03/2023 14:41 WG1982417
Naphthalene 0.362 0.0500 4 01/03/2023 14:41 WG1982417
n-Propylbenzene 0.0627 0.0200 4 01/03/2023 14:41 WG1982417
Styrene ND 0.0500 4 01/03/2023 14:41 WG1982417
1,1,1,2-Tetrachloroethane ND 0.0100 4 01/03/2023 14:41 WG1982417
1,1,2,2-Tetrachloroethane ND 0.0100 4 01/03/2023 14:41 WG1982417
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 01
L1570312
B1 (12-14)
Collected date/time: 12/21/22 10:25
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane ND 0.0100 4 01/03/2023 14:41 WG1982417
Tetrachloroethene ND 0.0100 4 01/03/2023 14:41 WG1982417
Toluene ND 0.0200 4 01/03/2023 14:41 WG1982417
1,2,3-Trichlorobenzene ND 0.0500 4 01/03/2023 14:41 WG1982417
1,2,4-Trichlorobenzene ND 0.0500 4 01/03/2023 14:41 WG1982417
1,1,1-Trichloroethane ND 0.0100 4 01/03/2023 14:41 WG1982417
1,1,2-Trichloroethane ND 0.0100 4 01/03/2023 14:41 WG1982417
Trichloroethene ND 0.00400 4 01/03/2023 14:41 WG1982417
Trichlorofluoromethane ND 0.0100 4 01/03/2023 14:41 WG1982417
1,2,3-Trichloropropane ND 0.0500 4 01/03/2023 14:41 WG1982417
1,2,4-Trimethylbenzene 0.0609 0.0200 4 01/03/2023 14:41 WG1982417
1,2,3-Trimethylbenzene ND 0.0200 4 01/03/2023 14:41 WG1982417
1,3,5-Trimethylbenzene ND 0.0200 4 01/03/2023 14:41 WG1982417
Vinyl chloride ND 0.0100 4 01/03/2023 14:41 WG1982417
Xylenes, Total ND 0.0260 4 01/03/2023 14:41 WG1982417
(S) Toluene-d8 98.6 75.0-131 01/03/2023 14:41 WG1982417
(S) 4-Bromofluorobenzene 103 67.0-138 01/03/2023 14:41 WG1982417
(S) 1,2-Dichloroethane-d4 92.7 70.0-130 01/03/2023 14:41 WG1982417
Sample Narrative:
L1570312-01 WG1982417: Non-target compounds too high to run at a lower dilution.
Semi-Volatile Organic Compounds (GC) by Method 8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 192 J3 J5 80.0 20 12/29/2022 14:49 WG1980058
(S) o-Terphenyl 0.000 J7 18.0-148 12/29/2022 14:49 WG1980058
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene 0.00845 0.00600 1 12/28/2022 17:36 WG1980069
Acenaphthene 0.133 0.00600 1 12/28/2022 17:36 WG1980069
Acenaphthylene 0.0337 0.00600 1 12/28/2022 17:36 WG1980069
Benzo(a)anthracene ND 0.00600 1 12/28/2022 17:36 WG1980069
Benzo(a)pyrene ND 0.00600 1 12/28/2022 17:36 WG1980069
Benzo(b)fluoranthene ND 0.00600 1 12/28/2022 17:36 WG1980069
Benzo(g,h,i)perylene ND 0.00600 1 12/28/2022 17:36 WG1980069
Benzo(k)fluoranthene ND 0.00600 1 12/28/2022 17:36 WG1980069
Chrysene ND 0.00600 1 12/28/2022 17:36 WG1980069
Dibenz(a,h)anthracene ND 0.00600 1 12/28/2022 17:36 WG1980069
Fluoranthene 0.00774 0.00600 1 12/28/2022 17:36 WG1980069
Fluorene 0.173 0.00600 1 12/28/2022 17:36 WG1980069
Indeno(1,2,3-cd)pyrene ND 0.00600 1 12/28/2022 17:36 WG1980069
Naphthalene 0.175 0.0200 1 12/28/2022 17:36 WG1980069
Phenanthrene 0.357 0.00600 1 12/28/2022 17:36 WG1980069
Pyrene 0.0181 0.00600 1 12/28/2022 17:36 WG1980069
1-Methylnaphthalene 0.969 0.0200 1 12/28/2022 17:36 WG1980069
2-Methylnaphthalene 1.30 0.0200 1 12/28/2022 17:36 WG1980069
2-Chloronaphthalene ND 0.0200 1 12/28/2022 17:36 WG1980069
(S) p-Terphenyl-d14 80.5 23.0-120 12/28/2022 17:36 WG1980069
(S) Nitrobenzene-d5 82.9 14.0-149 12/28/2022 17:36 WG1980069
(S) 2-Fluorobiphenyl 78.9 34.0-125 12/28/2022 17:36 WG1980069
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 02
L1570312
B1 (5-7)
Collected date/time: 12/21/22 10:25
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 77.1 1 12/29/2022 10:13 WG1980780
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 4.00 80 12/31/2022 19:47 WG1981849
Acrylonitrile ND 1.00 80 12/31/2022 19:47 WG1981849
Benzene ND 0.0800 80 12/31/2022 19:47 WG1981849
Bromobenzene ND J3 1.00 80 12/31/2022 19:47 WG1981849
Bromodichloromethane ND 0.200 80 12/31/2022 19:47 WG1981849
Bromoform ND 2.00 80 12/31/2022 19:47 WG1981849
Bromomethane ND 1.00 80 12/31/2022 19:47 WG1981849
n-Butylbenzene 1.41 1.00 80 12/31/2022 19:47 WG1981849
sec-Butylbenzene 1.18 1.00 80 12/31/2022 19:47 WG1981849
tert-Butylbenzene 0.575 J4 0.400 80 12/31/2022 19:47 WG1981849
Carbon tetrachloride ND 0.400 80 12/31/2022 19:47 WG1981849
Chlorobenzene ND 0.200 80 12/31/2022 19:47 WG1981849
Chlorodibromomethane ND 0.200 80 12/31/2022 19:47 WG1981849
Chloroethane ND 0.400 80 12/31/2022 19:47 WG1981849
Chloroform ND 0.200 80 12/31/2022 19:47 WG1981849
Chloromethane ND 1.00 80 12/31/2022 19:47 WG1981849
2-Chlorotoluene ND 0.200 80 12/31/2022 19:47 WG1981849
4-Chlorotoluene ND 0.400 80 12/31/2022 19:47 WG1981849
1,2-Dibromo-3-Chloropropane ND 2.00 80 12/31/2022 19:47 WG1981849
1,2-Dibromoethane ND 0.200 80 12/31/2022 19:47 WG1981849
Dibromomethane ND 0.400 80 12/31/2022 19:47 WG1981849
1,2-Dichlorobenzene ND 0.400 80 12/31/2022 19:47 WG1981849
1,3-Dichlorobenzene ND 0.400 80 12/31/2022 19:47 WG1981849
1,4-Dichlorobenzene ND 0.400 80 12/31/2022 19:47 WG1981849
Dichlorodifluoromethane ND 0.200 80 12/31/2022 19:47 WG1981849
1,1-Dichloroethane ND 0.200 80 12/31/2022 19:47 WG1981849
1,2-Dichloroethane ND 0.200 80 12/31/2022 19:47 WG1981849
1,1-Dichloroethene ND 0.200 80 12/31/2022 19:47 WG1981849
cis-1,2-Dichloroethene ND 0.200 80 12/31/2022 19:47 WG1981849
trans-1,2-Dichloroethene ND 0.400 80 12/31/2022 19:47 WG1981849
1,2-Dichloropropane ND 0.400 80 12/31/2022 19:47 WG1981849
1,1-Dichloropropene ND 0.200 80 12/31/2022 19:47 WG1981849
1,3-Dichloropropane ND 0.400 80 12/31/2022 19:47 WG1981849
cis-1,3-Dichloropropene ND J3 0.200 80 12/31/2022 19:47 WG1981849
trans-1,3-Dichloropropene ND 0.400 80 12/31/2022 19:47 WG1981849
2,2-Dichloropropane ND 0.200 80 12/31/2022 19:47 WG1981849
Di-isopropyl ether ND 0.0800 80 12/31/2022 19:47 WG1981849
Ethylbenzene 0.300 0.200 80 12/31/2022 19:47 WG1981849
Hexachloro-1,3-butadiene ND 2.00 80 12/31/2022 19:47 WG1981849
Isopropylbenzene 0.470 0.200 80 12/31/2022 19:47 WG1981849
p-Isopropyltoluene ND 0.400 80 12/31/2022 19:47 WG1981849
2-Butanone (MEK)ND 8.00 80 12/31/2022 19:47 WG1981849
Methylene Chloride ND 2.00 80 12/31/2022 19:47 WG1981849
4-Methyl-2-pentanone (MIBK)ND 2.00 80 12/31/2022 19:47 WG1981849
Methyl tert-butyl ether ND 0.0800 80 12/31/2022 19:47 WG1981849
Naphthalene 8.94 1.00 80 12/31/2022 19:47 WG1981849
n-Propylbenzene 0.732 0.400 80 12/31/2022 19:47 WG1981849
Styrene ND 1.00 80 12/31/2022 19:47 WG1981849
1,1,1,2-Tetrachloroethane ND 0.200 80 12/31/2022 19:47 WG1981849
1,1,2,2-Tetrachloroethane ND 0.200 80 12/31/2022 19:47 WG1981849
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 02
L1570312
B1 (5-7)
Collected date/time: 12/21/22 10:25
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane ND 0.200 80 12/31/2022 19:47 WG1981849
Tetrachloroethene ND 0.200 80 12/31/2022 19:47 WG1981849
Toluene ND 0.400 80 12/31/2022 19:47 WG1981849
1,2,3-Trichlorobenzene ND 1.00 80 12/31/2022 19:47 WG1981849
1,2,4-Trichlorobenzene ND 1.00 80 12/31/2022 19:47 WG1981849
1,1,1-Trichloroethane ND 0.200 80 12/31/2022 19:47 WG1981849
1,1,2-Trichloroethane ND 0.200 80 12/31/2022 19:47 WG1981849
Trichloroethene ND 0.0800 80 12/31/2022 19:47 WG1981849
Trichlorofluoromethane ND 0.200 80 12/31/2022 19:47 WG1981849
1,2,3-Trichloropropane ND 1.00 80 12/31/2022 19:47 WG1981849
1,2,4-Trimethylbenzene ND 0.400 80 12/31/2022 19:47 WG1981849
1,2,3-Trimethylbenzene ND 0.400 80 12/31/2022 19:47 WG1981849
1,3,5-Trimethylbenzene ND 0.400 80 12/31/2022 19:47 WG1981849
Vinyl chloride ND 0.200 80 12/31/2022 19:47 WG1981849
Xylenes, Total ND 0.520 80 12/31/2022 19:47 WG1981849
(S) Toluene-d8 100 75.0-131 12/31/2022 19:47 WG1981849
(S) 4-Bromofluorobenzene 116 67.0-138 12/31/2022 19:47 WG1981849
(S) 1,2-Dichloroethane-d4 94.4 70.0-130 12/31/2022 19:47 WG1981849
Sample Narrative:
L1570312-02 WG1981849: Non-target compounds too high to run at a lower dilution.
Semi-Volatile Organic Compounds (GC) by Method 8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 610 40.0 10 12/29/2022 13:57 WG1980058
(S) o-Terphenyl 129 18.0-148 12/29/2022 13:57 WG1980058
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene 0.163 J6 0.00600 1 12/28/2022 16:43 WG1980069
Acenaphthene 1.59 J3 V 0.00600 1 12/28/2022 16:43 WG1980069
Acenaphthylene ND J5 0.00600 1 12/28/2022 16:43 WG1980069
Benzo(a)anthracene 1.50 J3 V 0.00600 1 12/28/2022 16:43 WG1980069
Benzo(a)pyrene 1.26 J3 V 0.00600 1 12/28/2022 16:43 WG1980069
Benzo(b)fluoranthene 1.52 J3 V 0.00600 1 12/28/2022 16:43 WG1980069
Benzo(g,h,i)perylene 0.752 J3 V 0.00600 1 12/28/2022 16:43 WG1980069
Benzo(k)fluoranthene 0.556 J3 V 0.00600 1 12/28/2022 16:43 WG1980069
Chrysene 1.17 J3 V 0.00600 1 12/28/2022 16:43 WG1980069
Dibenz(a,h)anthracene 0.191 J3 J6 0.00600 1 12/28/2022 16:43 WG1980069
Fluoranthene 1.29 V 0.00600 1 12/28/2022 16:43 WG1980069
Fluorene 2.01 J3 V 0.00600 1 12/28/2022 16:43 WG1980069
Indeno(1,2,3-cd)pyrene 0.919 J3 V 0.00600 1 12/28/2022 16:43 WG1980069
Naphthalene 5.32 0.200 10 12/29/2022 22:34 WG1980069
Phenanthrene 2.74 V 0.00600 1 12/28/2022 16:43 WG1980069
Pyrene 1.14 V 0.00600 1 12/28/2022 16:43 WG1980069
1-Methylnaphthalene 11.2 0.200 10 12/29/2022 22:34 WG1980069
2-Methylnaphthalene 21.0 0.200 10 12/29/2022 22:34 WG1980069
2-Chloronaphthalene ND 0.0200 1 12/28/2022 16:43 WG1980069
(S) p-Terphenyl-d14 74.7 23.0-120 12/28/2022 16:43 WG1980069
(S) p-Terphenyl-d14 75.3 23.0-120 12/29/2022 22:34 WG1980069
(S) Nitrobenzene-d5 0.000 J2 14.0-149 12/28/2022 16:43 WG1980069
(S) Nitrobenzene-d5 0.000 J2 14.0-149 12/29/2022 22:34 WG1980069
(S) 2-Fluorobiphenyl 71.6 34.0-125 12/29/2022 22:34 WG1980069
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 02
L1570312
B1 (5-7)
Collected date/time: 12/21/22 10:25
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
(S) 2-Fluorobiphenyl 99.4 34.0-125 12/28/2022 16:43 WG1980069
Sample Narrative:
L1570312-02 WG1980069: Surrogate failure due to matrix interference
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 03
L1570312
B2 (6-8)
Collected date/time: 12/21/22 11:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 78.0 1 12/29/2022 10:13 WG1980780
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0500 1 12/31/2022 18:21 WG1981849
Acrylonitrile ND 0.0125 1 12/31/2022 18:21 WG1981849
Benzene ND 0.00100 1 12/31/2022 18:21 WG1981849
Bromobenzene ND J3 0.0125 1 12/31/2022 18:21 WG1981849
Bromodichloromethane ND 0.00250 1 12/31/2022 18:21 WG1981849
Bromoform ND 0.0250 1 12/31/2022 18:21 WG1981849
Bromomethane ND 0.0125 1 12/31/2022 18:21 WG1981849
n-Butylbenzene ND 0.0125 1 12/31/2022 18:21 WG1981849
sec-Butylbenzene ND 0.0125 1 12/31/2022 18:21 WG1981849
tert-Butylbenzene ND J4 0.00500 1 12/31/2022 18:21 WG1981849
Carbon tetrachloride ND 0.00500 1 12/31/2022 18:21 WG1981849
Chlorobenzene ND 0.00250 1 12/31/2022 18:21 WG1981849
Chlorodibromomethane ND 0.00250 1 12/31/2022 18:21 WG1981849
Chloroethane ND 0.00500 1 12/31/2022 18:21 WG1981849
Chloroform ND 0.00250 1 12/31/2022 18:21 WG1981849
Chloromethane ND 0.0125 1 12/31/2022 18:21 WG1981849
2-Chlorotoluene ND 0.00250 1 12/31/2022 18:21 WG1981849
4-Chlorotoluene ND 0.00500 1 12/31/2022 18:21 WG1981849
1,2-Dibromo-3-Chloropropane ND 0.0250 1 12/31/2022 18:21 WG1981849
1,2-Dibromoethane ND 0.00250 1 12/31/2022 18:21 WG1981849
Dibromomethane ND 0.00500 1 12/31/2022 18:21 WG1981849
1,2-Dichlorobenzene ND 0.00500 1 12/31/2022 18:21 WG1981849
1,3-Dichlorobenzene ND 0.00500 1 12/31/2022 18:21 WG1981849
1,4-Dichlorobenzene ND 0.00500 1 12/31/2022 18:21 WG1981849
Dichlorodifluoromethane ND 0.00250 1 12/31/2022 18:21 WG1981849
1,1-Dichloroethane ND 0.00250 1 12/31/2022 18:21 WG1981849
1,2-Dichloroethane ND 0.00250 1 12/31/2022 18:21 WG1981849
1,1-Dichloroethene ND 0.00250 1 12/31/2022 18:21 WG1981849
cis-1,2-Dichloroethene ND 0.00250 1 12/31/2022 18:21 WG1981849
trans-1,2-Dichloroethene ND 0.00500 1 12/31/2022 18:21 WG1981849
1,2-Dichloropropane ND 0.00500 1 12/31/2022 18:21 WG1981849
1,1-Dichloropropene ND 0.00250 1 12/31/2022 18:21 WG1981849
1,3-Dichloropropane ND 0.00500 1 12/31/2022 18:21 WG1981849
cis-1,3-Dichloropropene ND J3 0.00250 1 12/31/2022 18:21 WG1981849
trans-1,3-Dichloropropene ND 0.00500 1 12/31/2022 18:21 WG1981849
2,2-Dichloropropane ND 0.00250 1 12/31/2022 18:21 WG1981849
Di-isopropyl ether ND 0.00100 1 12/31/2022 18:21 WG1981849
Ethylbenzene ND 0.00250 1 12/31/2022 18:21 WG1981849
Hexachloro-1,3-butadiene ND 0.0250 1 12/31/2022 18:21 WG1981849
Isopropylbenzene ND 0.00250 1 12/31/2022 18:21 WG1981849
p-Isopropyltoluene ND 0.00500 1 12/31/2022 18:21 WG1981849
2-Butanone (MEK)ND 0.100 1 12/31/2022 18:21 WG1981849
Methylene Chloride ND 0.0250 1 12/31/2022 18:21 WG1981849
4-Methyl-2-pentanone (MIBK)ND 0.0250 1 12/31/2022 18:21 WG1981849
Methyl tert-butyl ether ND 0.00100 1 12/31/2022 18:21 WG1981849
Naphthalene ND 0.0125 1 12/31/2022 18:21 WG1981849
n-Propylbenzene ND 0.00500 1 12/31/2022 18:21 WG1981849
Styrene ND 0.0125 1 12/31/2022 18:21 WG1981849
1,1,1,2-Tetrachloroethane ND 0.00250 1 12/31/2022 18:21 WG1981849
1,1,2,2-Tetrachloroethane ND 0.00250 1 12/31/2022 18:21 WG1981849
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 03
L1570312
B2 (6-8)
Collected date/time: 12/21/22 11:10
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane ND 0.00250 1 12/31/2022 18:21 WG1981849
Tetrachloroethene ND 0.00250 1 12/31/2022 18:21 WG1981849
Toluene ND 0.00500 1 12/31/2022 18:21 WG1981849
1,2,3-Trichlorobenzene ND 0.0125 1 12/31/2022 18:21 WG1981849
1,2,4-Trichlorobenzene ND 0.0125 1 12/31/2022 18:21 WG1981849
1,1,1-Trichloroethane ND 0.00250 1 12/31/2022 18:21 WG1981849
1,1,2-Trichloroethane ND 0.00250 1 12/31/2022 18:21 WG1981849
Trichloroethene ND 0.00100 1 12/31/2022 18:21 WG1981849
Trichlorofluoromethane ND 0.00250 1 12/31/2022 18:21 WG1981849
1,2,3-Trichloropropane ND 0.0125 1 12/31/2022 18:21 WG1981849
1,2,4-Trimethylbenzene ND 0.00500 1 12/31/2022 18:21 WG1981849
1,2,3-Trimethylbenzene ND 0.00500 1 12/31/2022 18:21 WG1981849
1,3,5-Trimethylbenzene ND 0.00500 1 12/31/2022 18:21 WG1981849
Vinyl chloride ND 0.00250 1 12/31/2022 18:21 WG1981849
Xylenes, Total ND 0.00650 1 12/31/2022 18:21 WG1981849
(S) Toluene-d8 112 75.0-131 12/31/2022 18:21 WG1981849
(S) 4-Bromofluorobenzene 87.6 67.0-138 12/31/2022 18:21 WG1981849
(S) 1,2-Dichloroethane-d4 92.2 70.0-130 12/31/2022 18:21 WG1981849
Semi-Volatile Organic Compounds (GC) by Method 8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 9.90 4.00 1 12/29/2022 16:20 WG1980058
(S) o-Terphenyl 48.3 18.0-148 12/29/2022 16:20 WG1980058
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00600 1 12/28/2022 16:25 WG1980069
Acenaphthene ND 0.00600 1 12/28/2022 16:25 WG1980069
Acenaphthylene ND 0.00600 1 12/28/2022 16:25 WG1980069
Benzo(a)anthracene ND 0.00600 1 12/28/2022 16:25 WG1980069
Benzo(a)pyrene ND 0.00600 1 12/28/2022 16:25 WG1980069
Benzo(b)fluoranthene ND 0.00600 1 12/28/2022 16:25 WG1980069
Benzo(g,h,i)perylene ND 0.00600 1 12/28/2022 16:25 WG1980069
Benzo(k)fluoranthene ND 0.00600 1 12/28/2022 16:25 WG1980069
Chrysene ND 0.00600 1 12/28/2022 16:25 WG1980069
Dibenz(a,h)anthracene ND 0.00600 1 12/28/2022 16:25 WG1980069
Fluoranthene ND 0.00600 1 12/28/2022 16:25 WG1980069
Fluorene ND 0.00600 1 12/28/2022 16:25 WG1980069
Indeno(1,2,3-cd)pyrene ND 0.00600 1 12/28/2022 16:25 WG1980069
Naphthalene ND 0.0200 1 12/28/2022 16:25 WG1980069
Phenanthrene ND 0.00600 1 12/28/2022 16:25 WG1980069
Pyrene ND 0.00600 1 12/28/2022 16:25 WG1980069
1-Methylnaphthalene ND 0.0200 1 12/28/2022 16:25 WG1980069
2-Methylnaphthalene ND 0.0200 1 12/28/2022 16:25 WG1980069
2-Chloronaphthalene ND 0.0200 1 12/28/2022 16:25 WG1980069
(S) p-Terphenyl-d14 138 J1 23.0-120 12/28/2022 16:25 WG1980069
(S) Nitrobenzene-d5 146 14.0-149 12/28/2022 16:25 WG1980069
(S) 2-Fluorobiphenyl 124 34.0-125 12/28/2022 16:25 WG1980069
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 04
L1570312
B2 (17-19)
Collected date/time: 12/21/22 11:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 77.5 1 12/29/2022 10:13 WG1980780
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0500 1 12/31/2022 18:43 WG1981849
Acrylonitrile ND 0.0125 1 12/31/2022 18:43 WG1981849
Benzene ND 0.00100 1 12/31/2022 18:43 WG1981849
Bromobenzene ND J3 0.0125 1 12/31/2022 18:43 WG1981849
Bromodichloromethane ND 0.00250 1 12/31/2022 18:43 WG1981849
Bromoform ND 0.0250 1 12/31/2022 18:43 WG1981849
Bromomethane ND 0.0125 1 12/31/2022 18:43 WG1981849
n-Butylbenzene ND 0.0125 1 12/31/2022 18:43 WG1981849
sec-Butylbenzene ND 0.0125 1 12/31/2022 18:43 WG1981849
tert-Butylbenzene ND J4 0.00500 1 12/31/2022 18:43 WG1981849
Carbon tetrachloride ND 0.00500 1 12/31/2022 18:43 WG1981849
Chlorobenzene ND 0.00250 1 12/31/2022 18:43 WG1981849
Chlorodibromomethane ND 0.00250 1 12/31/2022 18:43 WG1981849
Chloroethane ND 0.00500 1 12/31/2022 18:43 WG1981849
Chloroform ND 0.00250 1 12/31/2022 18:43 WG1981849
Chloromethane ND 0.0125 1 12/31/2022 18:43 WG1981849
2-Chlorotoluene ND 0.00250 1 12/31/2022 18:43 WG1981849
4-Chlorotoluene ND 0.00500 1 12/31/2022 18:43 WG1981849
1,2-Dibromo-3-Chloropropane ND 0.0250 1 12/31/2022 18:43 WG1981849
1,2-Dibromoethane ND 0.00250 1 12/31/2022 18:43 WG1981849
Dibromomethane ND 0.00500 1 12/31/2022 18:43 WG1981849
1,2-Dichlorobenzene ND 0.00500 1 12/31/2022 18:43 WG1981849
1,3-Dichlorobenzene ND 0.00500 1 12/31/2022 18:43 WG1981849
1,4-Dichlorobenzene ND 0.00500 1 12/31/2022 18:43 WG1981849
Dichlorodifluoromethane ND 0.00250 1 12/31/2022 18:43 WG1981849
1,1-Dichloroethane ND 0.00250 1 12/31/2022 18:43 WG1981849
1,2-Dichloroethane ND 0.00250 1 12/31/2022 18:43 WG1981849
1,1-Dichloroethene ND 0.00250 1 12/31/2022 18:43 WG1981849
cis-1,2-Dichloroethene ND 0.00250 1 12/31/2022 18:43 WG1981849
trans-1,2-Dichloroethene ND 0.00500 1 12/31/2022 18:43 WG1981849
1,2-Dichloropropane ND 0.00500 1 12/31/2022 18:43 WG1981849
1,1-Dichloropropene ND 0.00250 1 12/31/2022 18:43 WG1981849
1,3-Dichloropropane ND 0.00500 1 12/31/2022 18:43 WG1981849
cis-1,3-Dichloropropene ND J3 0.00250 1 12/31/2022 18:43 WG1981849
trans-1,3-Dichloropropene ND 0.00500 1 12/31/2022 18:43 WG1981849
2,2-Dichloropropane ND 0.00250 1 12/31/2022 18:43 WG1981849
Di-isopropyl ether ND 0.00100 1 12/31/2022 18:43 WG1981849
Ethylbenzene ND 0.00250 1 12/31/2022 18:43 WG1981849
Hexachloro-1,3-butadiene ND 0.0250 1 12/31/2022 18:43 WG1981849
Isopropylbenzene ND 0.00250 1 12/31/2022 18:43 WG1981849
p-Isopropyltoluene ND 0.00500 1 12/31/2022 18:43 WG1981849
2-Butanone (MEK)ND 0.100 1 12/31/2022 18:43 WG1981849
Methylene Chloride ND 0.0250 1 12/31/2022 18:43 WG1981849
4-Methyl-2-pentanone (MIBK)ND 0.0250 1 12/31/2022 18:43 WG1981849
Methyl tert-butyl ether ND 0.00100 1 12/31/2022 18:43 WG1981849
Naphthalene 0.0196 0.0125 1 12/31/2022 18:43 WG1981849
n-Propylbenzene ND 0.00500 1 12/31/2022 18:43 WG1981849
Styrene ND 0.0125 1 12/31/2022 18:43 WG1981849
1,1,1,2-Tetrachloroethane ND 0.00250 1 12/31/2022 18:43 WG1981849
1,1,2,2-Tetrachloroethane ND 0.00250 1 12/31/2022 18:43 WG1981849
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 04
L1570312
B2 (17-19)
Collected date/time: 12/21/22 11:10
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane ND 0.00250 1 12/31/2022 18:43 WG1981849
Tetrachloroethene ND 0.00250 1 12/31/2022 18:43 WG1981849
Toluene ND 0.00500 1 12/31/2022 18:43 WG1981849
1,2,3-Trichlorobenzene ND 0.0125 1 12/31/2022 18:43 WG1981849
1,2,4-Trichlorobenzene ND 0.0125 1 12/31/2022 18:43 WG1981849
1,1,1-Trichloroethane ND 0.00250 1 12/31/2022 18:43 WG1981849
1,1,2-Trichloroethane ND 0.00250 1 12/31/2022 18:43 WG1981849
Trichloroethene ND 0.00100 1 12/31/2022 18:43 WG1981849
Trichlorofluoromethane ND 0.00250 1 12/31/2022 18:43 WG1981849
1,2,3-Trichloropropane ND 0.0125 1 12/31/2022 18:43 WG1981849
1,2,4-Trimethylbenzene 0.0169 0.00500 1 12/31/2022 18:43 WG1981849
1,2,3-Trimethylbenzene ND 0.00500 1 12/31/2022 18:43 WG1981849
1,3,5-Trimethylbenzene 0.00647 0.00500 1 12/31/2022 18:43 WG1981849
Vinyl chloride ND 0.00250 1 12/31/2022 18:43 WG1981849
Xylenes, Total ND 0.00650 1 12/31/2022 18:43 WG1981849
(S) Toluene-d8 110 75.0-131 12/31/2022 18:43 WG1981849
(S) 4-Bromofluorobenzene 91.6 67.0-138 12/31/2022 18:43 WG1981849
(S) 1,2-Dichloroethane-d4 97.5 70.0-130 12/31/2022 18:43 WG1981849
Semi-Volatile Organic Compounds (GC) by Method 8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 31.9 4.00 1 12/29/2022 11:47 WG1980058
(S) o-Terphenyl 41.6 18.0-148 12/29/2022 11:47 WG1980058
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene ND 0.00600 1 12/28/2022 13:10 WG1980069
Acenaphthene 0.0169 0.00600 1 12/28/2022 13:10 WG1980069
Acenaphthylene ND 0.00600 1 12/28/2022 13:10 WG1980069
Benzo(a)anthracene ND 0.00600 1 12/28/2022 13:10 WG1980069
Benzo(a)pyrene ND 0.00600 1 12/28/2022 13:10 WG1980069
Benzo(b)fluoranthene ND 0.00600 1 12/28/2022 13:10 WG1980069
Benzo(g,h,i)perylene ND 0.00600 1 12/28/2022 13:10 WG1980069
Benzo(k)fluoranthene ND 0.00600 1 12/28/2022 13:10 WG1980069
Chrysene ND 0.00600 1 12/28/2022 13:10 WG1980069
Dibenz(a,h)anthracene ND 0.00600 1 12/28/2022 13:10 WG1980069
Fluoranthene ND 0.00600 1 12/28/2022 13:10 WG1980069
Fluorene 0.0411 0.00600 1 12/28/2022 13:10 WG1980069
Indeno(1,2,3-cd)pyrene ND 0.00600 1 12/28/2022 13:10 WG1980069
Naphthalene ND 0.0200 1 12/28/2022 13:10 WG1980069
Phenanthrene 0.130 0.00600 1 12/28/2022 13:10 WG1980069
Pyrene ND 0.00600 1 12/28/2022 13:10 WG1980069
1-Methylnaphthalene 0.133 0.0200 1 12/28/2022 13:10 WG1980069
2-Methylnaphthalene 0.213 0.0200 1 12/28/2022 13:10 WG1980069
2-Chloronaphthalene ND 0.0200 1 12/28/2022 13:10 WG1980069
(S) p-Terphenyl-d14 69.5 23.0-120 12/28/2022 13:10 WG1980069
(S) Nitrobenzene-d5 80.3 14.0-149 12/28/2022 13:10 WG1980069
(S) 2-Fluorobiphenyl 52.9 34.0-125 12/28/2022 13:10 WG1980069
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 05
L1570312
B3 (6-8)
Collected date/time: 12/21/22 12:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 78.0 1 12/29/2022 10:13 WG1980780
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 4.00 80 12/31/2022 20:09 WG1981849
Acrylonitrile ND 1.00 80 12/31/2022 20:09 WG1981849
Benzene ND 0.0800 80 12/31/2022 20:09 WG1981849
Bromobenzene ND J3 1.00 80 12/31/2022 20:09 WG1981849
Bromodichloromethane ND 0.200 80 12/31/2022 20:09 WG1981849
Bromoform ND 2.00 80 12/31/2022 20:09 WG1981849
Bromomethane ND 1.00 80 12/31/2022 20:09 WG1981849
n-Butylbenzene 1.28 1.00 80 12/31/2022 20:09 WG1981849
sec-Butylbenzene 1.15 1.00 80 12/31/2022 20:09 WG1981849
tert-Butylbenzene ND J4 0.400 80 12/31/2022 20:09 WG1981849
Carbon tetrachloride ND 0.400 80 12/31/2022 20:09 WG1981849
Chlorobenzene ND 0.200 80 12/31/2022 20:09 WG1981849
Chlorodibromomethane ND 0.200 80 12/31/2022 20:09 WG1981849
Chloroethane ND 0.400 80 12/31/2022 20:09 WG1981849
Chloroform ND 0.200 80 12/31/2022 20:09 WG1981849
Chloromethane ND 1.00 80 12/31/2022 20:09 WG1981849
2-Chlorotoluene ND 0.200 80 12/31/2022 20:09 WG1981849
4-Chlorotoluene ND 0.400 80 12/31/2022 20:09 WG1981849
1,2-Dibromo-3-Chloropropane ND 2.00 80 12/31/2022 20:09 WG1981849
1,2-Dibromoethane ND 0.200 80 12/31/2022 20:09 WG1981849
Dibromomethane ND 0.400 80 12/31/2022 20:09 WG1981849
1,2-Dichlorobenzene ND 0.400 80 12/31/2022 20:09 WG1981849
1,3-Dichlorobenzene ND 0.400 80 12/31/2022 20:09 WG1981849
1,4-Dichlorobenzene ND 0.400 80 12/31/2022 20:09 WG1981849
Dichlorodifluoromethane ND 0.200 80 12/31/2022 20:09 WG1981849
1,1-Dichloroethane ND 0.200 80 12/31/2022 20:09 WG1981849
1,2-Dichloroethane ND 0.200 80 12/31/2022 20:09 WG1981849
1,1-Dichloroethene ND 0.200 80 12/31/2022 20:09 WG1981849
cis-1,2-Dichloroethene ND 0.200 80 12/31/2022 20:09 WG1981849
trans-1,2-Dichloroethene ND 0.400 80 12/31/2022 20:09 WG1981849
1,2-Dichloropropane ND 0.400 80 12/31/2022 20:09 WG1981849
1,1-Dichloropropene ND 0.200 80 12/31/2022 20:09 WG1981849
1,3-Dichloropropane ND 0.400 80 12/31/2022 20:09 WG1981849
cis-1,3-Dichloropropene ND J3 0.200 80 12/31/2022 20:09 WG1981849
trans-1,3-Dichloropropene ND 0.400 80 12/31/2022 20:09 WG1981849
2,2-Dichloropropane ND 0.200 80 12/31/2022 20:09 WG1981849
Di-isopropyl ether ND 0.0800 80 12/31/2022 20:09 WG1981849
Ethylbenzene 0.390 0.200 80 12/31/2022 20:09 WG1981849
Hexachloro-1,3-butadiene ND 2.00 80 12/31/2022 20:09 WG1981849
Isopropylbenzene 0.743 0.200 80 12/31/2022 20:09 WG1981849
p-Isopropyltoluene ND 0.400 80 12/31/2022 20:09 WG1981849
2-Butanone (MEK)ND 8.00 80 12/31/2022 20:09 WG1981849
Methylene Chloride ND 2.00 80 12/31/2022 20:09 WG1981849
4-Methyl-2-pentanone (MIBK)ND 2.00 80 12/31/2022 20:09 WG1981849
Methyl tert-butyl ether ND 0.0800 80 12/31/2022 20:09 WG1981849
Naphthalene 3.98 1.00 80 12/31/2022 20:09 WG1981849
n-Propylbenzene 1.11 0.400 80 12/31/2022 20:09 WG1981849
Styrene ND 1.00 80 12/31/2022 20:09 WG1981849
1,1,1,2-Tetrachloroethane ND 0.200 80 12/31/2022 20:09 WG1981849
1,1,2,2-Tetrachloroethane ND 0.200 80 12/31/2022 20:09 WG1981849
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 05
L1570312
B3 (6-8)
Collected date/time: 12/21/22 12:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane ND 0.200 80 12/31/2022 20:09 WG1981849
Tetrachloroethene ND 0.200 80 12/31/2022 20:09 WG1981849
Toluene ND 0.400 80 12/31/2022 20:09 WG1981849
1,2,3-Trichlorobenzene ND 1.00 80 12/31/2022 20:09 WG1981849
1,2,4-Trichlorobenzene ND 1.00 80 12/31/2022 20:09 WG1981849
1,1,1-Trichloroethane ND 0.200 80 12/31/2022 20:09 WG1981849
1,1,2-Trichloroethane ND 0.200 80 12/31/2022 20:09 WG1981849
Trichloroethene ND 0.0800 80 12/31/2022 20:09 WG1981849
Trichlorofluoromethane ND 0.200 80 12/31/2022 20:09 WG1981849
1,2,3-Trichloropropane ND 1.00 80 12/31/2022 20:09 WG1981849
1,2,4-Trimethylbenzene ND 0.400 80 12/31/2022 20:09 WG1981849
1,2,3-Trimethylbenzene ND 0.400 80 12/31/2022 20:09 WG1981849
1,3,5-Trimethylbenzene ND 0.400 80 12/31/2022 20:09 WG1981849
Vinyl chloride ND 0.200 80 12/31/2022 20:09 WG1981849
Xylenes, Total ND 0.520 80 12/31/2022 20:09 WG1981849
(S) Toluene-d8 105 75.0-131 12/31/2022 20:09 WG1981849
(S) 4-Bromofluorobenzene 112 67.0-138 12/31/2022 20:09 WG1981849
(S) 1,2-Dichloroethane-d4 95.1 70.0-130 12/31/2022 20:09 WG1981849
Sample Narrative:
L1570312-05 WG1981849: Non-target compounds too high to run at a lower dilution.
Semi-Volatile Organic Compounds (GC) by Method 8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 987 40.0 10 12/29/2022 14:23 WG1980058
(S) o-Terphenyl 156 J1 18.0-148 12/29/2022 14:23 WG1980058
Sample Narrative:
L1570312-05 WG1980058: Surrogate failure due to matrix interference
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene 0.0648 0.00600 1 12/28/2022 15:50 WG1980069
Acenaphthene 0.746 0.00600 1 12/28/2022 15:50 WG1980069
Acenaphthylene ND 0.00600 1 12/28/2022 15:50 WG1980069
Benzo(a)anthracene ND 0.00600 1 12/28/2022 15:50 WG1980069
Benzo(a)pyrene ND 0.00600 1 12/28/2022 15:50 WG1980069
Benzo(b)fluoranthene ND 0.00600 1 12/28/2022 15:50 WG1980069
Benzo(g,h,i)perylene ND 0.00600 1 12/28/2022 15:50 WG1980069
Benzo(k)fluoranthene ND 0.00600 1 12/28/2022 15:50 WG1980069
Chrysene ND 0.00600 1 12/28/2022 15:50 WG1980069
Dibenz(a,h)anthracene ND 0.00600 1 12/28/2022 15:50 WG1980069
Fluoranthene 0.0501 0.00600 1 12/28/2022 15:50 WG1980069
Fluorene 1.00 0.00600 1 12/28/2022 15:50 WG1980069
Indeno(1,2,3-cd)pyrene ND 0.00600 1 12/28/2022 15:50 WG1980069
Naphthalene 1.83 0.0200 1 12/28/2022 15:50 WG1980069
Phenanthrene 1.82 0.00600 1 12/28/2022 15:50 WG1980069
Pyrene 0.186 0.00600 1 12/28/2022 15:50 WG1980069
1-Methylnaphthalene 4.72 0.100 5 12/29/2022 21:23 WG1980069
2-Methylnaphthalene 7.89 0.100 5 12/29/2022 21:23 WG1980069
2-Chloronaphthalene ND 0.0200 1 12/28/2022 15:50 WG1980069
(S) p-Terphenyl-d14 82.8 23.0-120 12/29/2022 21:23 WG1980069
(S) p-Terphenyl-d14 79.3 23.0-120 12/28/2022 15:50 WG1980069
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
EBI Consulting EBICONPAZ-1222000463 L1570312 01/05/23 15:40 15 of 34
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
EBI Consulting EBICONPAZ-1222000463 L1570312 01/05/23 16:02 15 of 34
SAMPLE RESULTS - 05
L1570312
B3 (6-8)
Collected date/time: 12/21/22 12:20
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
(S) Nitrobenzene-d5 0.000 J2 14.0-149 12/28/2022 15:50 WG1980069
(S) Nitrobenzene-d5 0.000 J2 14.0-149 12/29/2022 21:23 WG1980069
(S) 2-Fluorobiphenyl 73.6 34.0-125 12/29/2022 21:23 WG1980069
(S) 2-Fluorobiphenyl 75.9 34.0-125 12/28/2022 15:50 WG1980069
Sample Narrative:
L1570312-05 WG1980069: Surrogate failure due to matrix interference
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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EBI Consulting EBICONPAZ-1222000463 L1570312 01/05/23 16:02 16 of 34
SAMPLE RESULTS - 06
L1570312
B3 (12-14)
Collected date/time: 12/21/22 12:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 74.2 1 12/29/2022 10:13 WG1980780
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 4.00 80 12/31/2022 20:30 WG1981849
Acrylonitrile ND 1.00 80 12/31/2022 20:30 WG1981849
Benzene ND 0.0800 80 12/31/2022 20:30 WG1981849
Bromobenzene ND J3 1.00 80 12/31/2022 20:30 WG1981849
Bromodichloromethane ND 0.200 80 12/31/2022 20:30 WG1981849
Bromoform ND 2.00 80 12/31/2022 20:30 WG1981849
Bromomethane ND 1.00 80 12/31/2022 20:30 WG1981849
n-Butylbenzene 1.53 1.00 80 12/31/2022 20:30 WG1981849
sec-Butylbenzene 1.27 1.00 80 12/31/2022 20:30 WG1981849
tert-Butylbenzene ND J4 0.400 80 12/31/2022 20:30 WG1981849
Carbon tetrachloride ND 0.400 80 12/31/2022 20:30 WG1981849
Chlorobenzene ND 0.200 80 12/31/2022 20:30 WG1981849
Chlorodibromomethane ND 0.200 80 12/31/2022 20:30 WG1981849
Chloroethane ND 0.400 80 12/31/2022 20:30 WG1981849
Chloroform ND 0.200 80 12/31/2022 20:30 WG1981849
Chloromethane ND 1.00 80 12/31/2022 20:30 WG1981849
2-Chlorotoluene ND 0.200 80 12/31/2022 20:30 WG1981849
4-Chlorotoluene ND 0.400 80 12/31/2022 20:30 WG1981849
1,2-Dibromo-3-Chloropropane ND 2.00 80 12/31/2022 20:30 WG1981849
1,2-Dibromoethane ND 0.200 80 12/31/2022 20:30 WG1981849
Dibromomethane ND 0.400 80 12/31/2022 20:30 WG1981849
1,2-Dichlorobenzene ND 0.400 80 12/31/2022 20:30 WG1981849
1,3-Dichlorobenzene ND 0.400 80 12/31/2022 20:30 WG1981849
1,4-Dichlorobenzene ND 0.400 80 12/31/2022 20:30 WG1981849
Dichlorodifluoromethane ND 0.200 80 12/31/2022 20:30 WG1981849
1,1-Dichloroethane ND 0.200 80 12/31/2022 20:30 WG1981849
1,2-Dichloroethane ND 0.200 80 12/31/2022 20:30 WG1981849
1,1-Dichloroethene ND 0.200 80 12/31/2022 20:30 WG1981849
cis-1,2-Dichloroethene ND 0.200 80 12/31/2022 20:30 WG1981849
trans-1,2-Dichloroethene ND 0.400 80 12/31/2022 20:30 WG1981849
1,2-Dichloropropane ND 0.400 80 12/31/2022 20:30 WG1981849
1,1-Dichloropropene ND 0.200 80 12/31/2022 20:30 WG1981849
1,3-Dichloropropane ND 0.400 80 12/31/2022 20:30 WG1981849
cis-1,3-Dichloropropene ND J3 0.200 80 12/31/2022 20:30 WG1981849
trans-1,3-Dichloropropene ND 0.400 80 12/31/2022 20:30 WG1981849
2,2-Dichloropropane ND 0.200 80 12/31/2022 20:30 WG1981849
Di-isopropyl ether ND 0.0800 80 12/31/2022 20:30 WG1981849
Ethylbenzene 0.825 0.200 80 12/31/2022 20:30 WG1981849
Hexachloro-1,3-butadiene ND 2.00 80 12/31/2022 20:30 WG1981849
Isopropylbenzene 0.831 0.200 80 12/31/2022 20:30 WG1981849
p-Isopropyltoluene ND 0.400 80 12/31/2022 20:30 WG1981849
2-Butanone (MEK)ND 8.00 80 12/31/2022 20:30 WG1981849
Methylene Chloride ND 2.00 80 12/31/2022 20:30 WG1981849
4-Methyl-2-pentanone (MIBK)ND 2.00 80 12/31/2022 20:30 WG1981849
Methyl tert-butyl ether ND 0.0800 80 12/31/2022 20:30 WG1981849
Naphthalene 1.88 1.00 80 12/31/2022 20:30 WG1981849
n-Propylbenzene 1.24 0.400 80 12/31/2022 20:30 WG1981849
Styrene ND 1.00 80 12/31/2022 20:30 WG1981849
1,1,1,2-Tetrachloroethane ND 0.200 80 12/31/2022 20:30 WG1981849
1,1,2,2-Tetrachloroethane ND 0.200 80 12/31/2022 20:30 WG1981849
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 06
L1570312
B3 (12-14)
Collected date/time: 12/21/22 12:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane ND 0.200 80 12/31/2022 20:30 WG1981849
Tetrachloroethene ND 0.200 80 12/31/2022 20:30 WG1981849
Toluene ND 0.400 80 12/31/2022 20:30 WG1981849
1,2,3-Trichlorobenzene ND 1.00 80 12/31/2022 20:30 WG1981849
1,2,4-Trichlorobenzene ND 1.00 80 12/31/2022 20:30 WG1981849
1,1,1-Trichloroethane ND 0.200 80 12/31/2022 20:30 WG1981849
1,1,2-Trichloroethane ND 0.200 80 12/31/2022 20:30 WG1981849
Trichloroethene ND 0.0800 80 12/31/2022 20:30 WG1981849
Trichlorofluoromethane ND 0.200 80 12/31/2022 20:30 WG1981849
1,2,3-Trichloropropane ND 1.00 80 12/31/2022 20:30 WG1981849
1,2,4-Trimethylbenzene ND 0.400 80 12/31/2022 20:30 WG1981849
1,2,3-Trimethylbenzene ND 0.400 80 12/31/2022 20:30 WG1981849
1,3,5-Trimethylbenzene ND 0.400 80 12/31/2022 20:30 WG1981849
Vinyl chloride ND 0.200 80 12/31/2022 20:30 WG1981849
Xylenes, Total ND 0.520 80 12/31/2022 20:30 WG1981849
(S) Toluene-d8 102 75.0-131 12/31/2022 20:30 WG1981849
(S) 4-Bromofluorobenzene 110 67.0-138 12/31/2022 20:30 WG1981849
(S) 1,2-Dichloroethane-d4 95.7 70.0-130 12/31/2022 20:30 WG1981849
Sample Narrative:
L1570312-06 WG1981849: Non-target compounds too high to run at a lower dilution.
Semi-Volatile Organic Compounds (GC) by Method 8015
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 734 40.0 10 12/29/2022 14:36 WG1980058
(S) o-Terphenyl 123 18.0-148 12/29/2022 14:36 WG1980058
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Anthracene 0.0672 0.00600 1 12/28/2022 15:32 WG1980069
Acenaphthene 0.572 0.00600 1 12/28/2022 15:32 WG1980069
Acenaphthylene ND 0.00600 1 12/28/2022 15:32 WG1980069
Benzo(a)anthracene ND 0.00600 1 12/28/2022 15:32 WG1980069
Benzo(a)pyrene ND 0.00600 1 12/28/2022 15:32 WG1980069
Benzo(b)fluoranthene ND 0.00600 1 12/28/2022 15:32 WG1980069
Benzo(g,h,i)perylene ND 0.00600 1 12/28/2022 15:32 WG1980069
Benzo(k)fluoranthene ND 0.00600 1 12/28/2022 15:32 WG1980069
Chrysene ND 0.00600 1 12/28/2022 15:32 WG1980069
Dibenz(a,h)anthracene ND 0.00600 1 12/28/2022 15:32 WG1980069
Fluoranthene 0.0414 0.00600 1 12/28/2022 15:32 WG1980069
Fluorene 0.793 0.00600 1 12/28/2022 15:32 WG1980069
Indeno(1,2,3-cd)pyrene ND 0.00600 1 12/28/2022 15:32 WG1980069
Naphthalene 0.502 0.0200 1 12/28/2022 15:32 WG1980069
Phenanthrene 1.62 0.00600 1 12/28/2022 15:32 WG1980069
Pyrene 0.157 0.00600 1 12/28/2022 15:32 WG1980069
1-Methylnaphthalene 3.10 0.0200 1 12/28/2022 15:32 WG1980069
2-Methylnaphthalene 2.63 0.0200 1 12/28/2022 15:32 WG1980069
2-Chloronaphthalene ND 0.0200 1 12/28/2022 15:32 WG1980069
(S) p-Terphenyl-d14 60.0 23.0-120 12/28/2022 15:32 WG1980069
(S) Nitrobenzene-d5 29.5 14.0-149 12/28/2022 15:32 WG1980069
(S) 2-Fluorobiphenyl 65.4 34.0-125 12/28/2022 15:32 WG1980069
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1980780
Total Solids by Method 2540 G-2011 L1570312-01,02,03,04,05,06
Method Blank (MB)
(MB) R3876708-1 12/29/22 10:13
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00200
L1570250-19 Original Sample (OS) • Duplicate (DUP)
(OS) L1570250-19 12/29/22 10:13 • (DUP) R3876708-3 12/29/22 10:13
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 80.8 77.0 1 4.77 10
Laboratory Control Sample (LCS)
(LCS) R3876708-2 12/29/22 10:13
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1981849
Volatile Organic Compounds (GC/MS) by Method 8260B L1570312-02,03,04,05,06
Method Blank (MB)
(MB) R3877399-3 12/31/22 13:34
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1981849
Volatile Organic Compounds (GC/MS) by Method 8260B L1570312-02,03,04,05,06
Method Blank (MB)
(MB) R3877399-3 12/31/22 13:34
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK)U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene 0.00253 J 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 113 75.0-131
(S) 4-Bromofluorobenzene 95.7 67.0-138
(S) 1,2-Dichloroethane-d4 92.1 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3877399-1 12/31/22 12:09 • (LCSD) R3877399-2 12/31/22 12:30
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 0.686 0.654 110 105 10.0-160 4.78 31
Acrylonitrile 0.625 0.639 0.630 102 101 45.0-153 1.42 22
Benzene 0.125 0.123 0.128 98.4 102 70.0-123 3.98 20
Bromobenzene 0.125 0.117 0.148 93.6 118 73.0-121 J3 23.4 20
Bromodichloromethane 0.125 0.119 0.131 95.2 105 73.0-121 9.60 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1981849
Volatile Organic Compounds (GC/MS) by Method 8260B L1570312-02,03,04,05,06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3877399-1 12/31/22 12:09 • (LCSD) R3877399-2 12/31/22 12:30
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.125 0.115 0.130 92.0 104 64.0-132 12.2 20
Bromomethane 0.125 0.130 0.129 104 103 56.0-147 0.772 20
n-Butylbenzene 0.125 0.125 0.132 100 106 68.0-135 5.45 20
sec-Butylbenzene 0.125 0.0993 0.0950 79.4 76.0 74.0-130 4.43 20
tert-Butylbenzene 0.125 0.0952 0.0935 76.2 74.8 75.0-127 J4 1.80 20
Carbon tetrachloride 0.125 0.134 0.141 107 113 66.0-128 5.09 20
Chlorobenzene 0.125 0.118 0.124 94.4 99.2 76.0-128 4.96 20
Chlorodibromomethane 0.125 0.115 0.124 92.0 99.2 74.0-127 7.53 20
Chloroethane 0.125 0.145 0.145 116 116 61.0-134 0.000 20
Chloroform 0.125 0.121 0.124 96.8 99.2 72.0-123 2.45 20
Chloromethane 0.125 0.134 0.132 107 106 51.0-138 1.50 20
2-Chlorotoluene 0.125 0.102 0.106 81.6 84.8 75.0-124 3.85 20
4-Chlorotoluene 0.125 0.116 0.132 92.8 106 75.0-124 12.9 20
1,2-Dibromo-3-Chloropropane 0.125 0.139 0.127 111 102 59.0-130 9.02 20
1,2-Dibromoethane 0.125 0.115 0.129 92.0 103 74.0-128 11.5 20
Dibromomethane 0.125 0.121 0.138 96.8 110 75.0-122 13.1 20
1,2-Dichlorobenzene 0.125 0.130 0.131 104 105 76.0-124 0.766 20
1,3-Dichlorobenzene 0.125 0.122 0.125 97.6 100 76.0-125 2.43 20
1,4-Dichlorobenzene 0.125 0.109 0.123 87.2 98.4 77.0-121 12.1 20
Dichlorodifluoromethane 0.125 0.137 0.144 110 115 43.0-156 4.98 20
1,1-Dichloroethane 0.125 0.119 0.127 95.2 102 70.0-127 6.50 20
1,2-Dichloroethane 0.125 0.122 0.125 97.6 100 65.0-131 2.43 20
1,1-Dichloroethene 0.125 0.128 0.131 102 105 65.0-131 2.32 20
cis-1,2-Dichloroethene 0.125 0.121 0.129 96.8 103 73.0-125 6.40 20
trans-1,2-Dichloroethene 0.125 0.121 0.123 96.8 98.4 71.0-125 1.64 20
1,2-Dichloropropane 0.125 0.115 0.127 92.0 102 74.0-125 9.92 20
1,1-Dichloropropene 0.125 0.117 0.129 93.6 103 73.0-125 9.76 20
1,3-Dichloropropane 0.125 0.125 0.139 100 111 80.0-125 10.6 20
cis-1,3-Dichloropropene 0.125 0.107 0.135 85.6 108 76.0-127 J3 23.1 20
trans-1,3-Dichloropropene 0.125 0.122 0.123 97.6 98.4 73.0-127 0.816 20
2,2-Dichloropropane 0.125 0.124 0.130 99.2 104 59.0-135 4.72 20
Di-isopropyl ether 0.125 0.123 0.128 98.4 102 60.0-136 3.98 20
Ethylbenzene 0.125 0.114 0.130 91.2 104 74.0-126 13.1 20
Hexachloro-1,3-butadiene 0.125 0.106 0.117 84.8 93.6 57.0-150 9.87 20
Isopropylbenzene 0.125 0.126 0.132 101 106 72.0-127 4.65 20
p-Isopropyltoluene 0.125 0.0983 0.0985 78.6 78.8 72.0-133 0.203 20
2-Butanone (MEK)0.625 0.591 0.714 94.6 114 30.0-160 18.9 24
Methylene Chloride 0.125 0.133 0.121 106 96.8 68.0-123 9.45 20
4-Methyl-2-pentanone (MIBK)0.625 0.607 0.588 97.1 94.1 56.0-143 3.18 20
Methyl tert-butyl ether 0.125 0.123 0.122 98.4 97.6 66.0-132 0.816 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1981849
Volatile Organic Compounds (GC/MS) by Method 8260B L1570312-02,03,04,05,06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3877399-1 12/31/22 12:09 • (LCSD) R3877399-2 12/31/22 12:30
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.125 0.142 0.134 114 107 59.0-130 5.80 20
n-Propylbenzene 0.125 0.101 0.107 80.8 85.6 74.0-126 5.77 20
Styrene 0.125 0.107 0.125 85.6 100 72.0-127 15.5 20
1,1,1,2-Tetrachloroethane 0.125 0.138 0.133 110 106 74.0-129 3.69 20
1,1,2,2-Tetrachloroethane 0.125 0.127 0.134 102 107 68.0-128 5.36 20
1,1,2-Trichlorotrifluoroethane 0.125 0.126 0.129 101 103 61.0-139 2.35 20
Tetrachloroethene 0.125 0.130 0.132 104 106 70.0-136 1.53 20
Toluene 0.125 0.119 0.126 95.2 101 75.0-121 5.71 20
1,2,3-Trichlorobenzene 0.125 0.145 0.133 116 106 59.0-139 8.63 20
1,2,4-Trichlorobenzene 0.125 0.140 0.136 112 109 62.0-137 2.90 20
1,1,1-Trichloroethane 0.125 0.134 0.133 107 106 69.0-126 0.749 20
1,1,2-Trichloroethane 0.125 0.124 0.125 99.2 100 78.0-123 0.803 20
Trichloroethene 0.125 0.120 0.126 96.0 101 76.0-126 4.88 20
Trichlorofluoromethane 0.125 0.130 0.134 104 107 61.0-142 3.03 20
1,2,3-Trichloropropane 0.125 0.113 0.118 90.4 94.4 67.0-129 4.33 20
1,2,4-Trimethylbenzene 0.125 0.101 0.104 80.8 83.2 70.0-126 2.93 20
1,2,3-Trimethylbenzene 0.125 0.107 0.104 85.6 83.2 74.0-124 2.84 20
1,3,5-Trimethylbenzene 0.125 0.104 0.104 83.2 83.2 73.0-127 0.000 20
Vinyl chloride 0.125 0.139 0.137 111 110 63.0-134 1.45 20
Xylenes, Total 0.375 0.364 0.391 97.1 104 72.0-127 7.15 20
(S) Toluene-d8 103 99.4 75.0-131
(S) 4-Bromofluorobenzene 89.2 99.0 67.0-138
(S) 1,2-Dichloroethane-d4 101 101 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1982417
Volatile Organic Compounds (GC/MS) by Method 8260B L1570312-01
Method Blank (MB)
(MB) R3878236-2 01/03/23 08:48
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1982417
Volatile Organic Compounds (GC/MS) by Method 8260B L1570312-01
Method Blank (MB)
(MB) R3878236-2 01/03/23 08:48
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK)U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene 0.00168 J 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 100 75.0-131
(S) 4-Bromofluorobenzene 97.8 67.0-138
(S) 1,2-Dichloroethane-d4 84.4 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3878236-1 01/03/23 07:52
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acetone 0.625 0.978 156 10.0-160
Acrylonitrile 0.625 0.614 98.2 45.0-153
Benzene 0.125 0.132 106 70.0-123
Bromobenzene 0.125 0.126 101 73.0-121
Bromodichloromethane 0.125 0.142 114 73.0-121
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1982417
Volatile Organic Compounds (GC/MS) by Method 8260B L1570312-01
Laboratory Control Sample (LCS)
(LCS) R3878236-1 01/03/23 07:52
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Bromoform 0.125 0.134 107 64.0-132
Bromomethane 0.125 0.0612 49.0 56.0-147 J4
n-Butylbenzene 0.125 0.112 89.6 68.0-135
sec-Butylbenzene 0.125 0.121 96.8 74.0-130
tert-Butylbenzene 0.125 0.125 100 75.0-127
Carbon tetrachloride 0.125 0.139 111 66.0-128
Chlorobenzene 0.125 0.130 104 76.0-128
Chlorodibromomethane 0.125 0.145 116 74.0-127
Chloroethane 0.125 0.104 83.2 61.0-134
Chloroform 0.125 0.149 119 72.0-123
Chloromethane 0.125 0.115 92.0 51.0-138
2-Chlorotoluene 0.125 0.120 96.0 75.0-124
4-Chlorotoluene 0.125 0.111 88.8 75.0-124
1,2-Dibromo-3-Chloropropane 0.125 0.113 90.4 59.0-130
1,2-Dibromoethane 0.125 0.131 105 74.0-128
Dibromomethane 0.125 0.138 110 75.0-122
1,2-Dichlorobenzene 0.125 0.133 106 76.0-124
1,3-Dichlorobenzene 0.125 0.130 104 76.0-125
1,4-Dichlorobenzene 0.125 0.125 100 77.0-121
Dichlorodifluoromethane 0.125 0.100 80.0 43.0-156
1,1-Dichloroethane 0.125 0.136 109 70.0-127
1,2-Dichloroethane 0.125 0.124 99.2 65.0-131
1,1-Dichloroethene 0.125 0.124 99.2 65.0-131
cis-1,2-Dichloroethene 0.125 0.140 112 73.0-125
trans-1,2-Dichloroethene 0.125 0.135 108 71.0-125
1,2-Dichloropropane 0.125 0.138 110 74.0-125
1,1-Dichloropropene 0.125 0.127 102 73.0-125
1,3-Dichloropropane 0.125 0.127 102 80.0-125
cis-1,3-Dichloropropene 0.125 0.139 111 76.0-127
trans-1,3-Dichloropropene 0.125 0.134 107 73.0-127
2,2-Dichloropropane 0.125 0.113 90.4 59.0-135
Di-isopropyl ether 0.125 0.120 96.0 60.0-136
Ethylbenzene 0.125 0.129 103 74.0-126
Hexachloro-1,3-butadiene 0.125 0.134 107 57.0-150
Isopropylbenzene 0.125 0.130 104 72.0-127
p-Isopropyltoluene 0.125 0.118 94.4 72.0-133
2-Butanone (MEK)0.625 0.649 104 30.0-160
Methylene Chloride 0.125 0.134 107 68.0-123
4-Methyl-2-pentanone (MIBK)0.625 0.600 96.0 56.0-143
Methyl tert-butyl ether 0.125 0.155 124 66.0-132
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1982417
Volatile Organic Compounds (GC/MS) by Method 8260B L1570312-01
Laboratory Control Sample (LCS)
(LCS) R3878236-1 01/03/23 07:52
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Naphthalene 0.125 0.119 95.2 59.0-130
n-Propylbenzene 0.125 0.115 92.0 74.0-126
Styrene 0.125 0.127 102 72.0-127
1,1,1,2-Tetrachloroethane 0.125 0.139 111 74.0-129
1,1,2,2-Tetrachloroethane 0.125 0.118 94.4 68.0-128
1,1,2-Trichlorotrifluoroethane 0.125 0.112 89.6 61.0-139
Tetrachloroethene 0.125 0.126 101 70.0-136
Toluene 0.125 0.126 101 75.0-121
1,2,3-Trichlorobenzene 0.125 0.133 106 59.0-139
1,2,4-Trichlorobenzene 0.125 0.136 109 62.0-137
1,1,1-Trichloroethane 0.125 0.144 115 69.0-126
1,1,2-Trichloroethane 0.125 0.136 109 78.0-123
Trichloroethene 0.125 0.148 118 76.0-126
Trichlorofluoromethane 0.125 0.118 94.4 61.0-142
1,2,3-Trichloropropane 0.125 0.138 110 67.0-129
1,2,4-Trimethylbenzene 0.125 0.121 96.8 70.0-126
1,2,3-Trimethylbenzene 0.125 0.127 102 74.0-124
1,3,5-Trimethylbenzene 0.125 0.126 101 73.0-127
Vinyl chloride 0.125 0.104 83.2 63.0-134
Xylenes, Total 0.375 0.388 103 72.0-127
(S) Toluene-d8 96.9 75.0-131
(S) 4-Bromofluorobenzene 97.4 67.0-138
(S) 1,2-Dichloroethane-d4 95.8 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1980058
Semi-Volatile Organic Compounds (GC) by Method 8015 L1570312-01,02,03,04,05,06
Method Blank (MB)
(MB) R3876593-1 12/29/22 10:16
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction U 0.769 4.00
(S) o-Terphenyl 67.6 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3876593-2 12/29/22 10:29
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) High Fraction 50.0 33.8 67.6 50.0-150
(S) o-Terphenyl 66.4 18.0-148
L1570312-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1570312-01 12/29/22 14:49 • (MS) R3876593-3 12/29/22 15:02 • (MSD) R3876593-4 12/29/22 15:15
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) High Fraction 50.0 192 233 292 82.0 200 20 50.0-150 J3 J5 22.5 20
(S) o-Terphenyl 0.000 0.000 18.0-148 J7 J7
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1980069
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1570312-01,02,03,04,05,06
Method Blank (MB)
(MB) R3876461-2 12/28/22 12:53
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00230 0.00600
Acenaphthene U 0.00209 0.00600
Acenaphthylene U 0.00216 0.00600
Benzo(a)anthracene U 0.00173 0.00600
Benzo(a)pyrene U 0.00179 0.00600
Benzo(b)fluoranthene U 0.00153 0.00600
Benzo(g,h,i)perylene U 0.00177 0.00600
Benzo(k)fluoranthene U 0.00215 0.00600
Chrysene U 0.00232 0.00600
Dibenz(a,h)anthracene U 0.00172 0.00600
Fluoranthene U 0.00227 0.00600
Fluorene U 0.00205 0.00600
Indeno(1,2,3-cd)pyrene U 0.00181 0.00600
Naphthalene U 0.00408 0.0200
Phenanthrene U 0.00231 0.00600
Pyrene U 0.00200 0.00600
1-Methylnaphthalene U 0.00449 0.0200
2-Methylnaphthalene U 0.00427 0.0200
2-Chloronaphthalene U 0.00466 0.0200
(S) p-Terphenyl-d14 86.7 23.0-120
(S) Nitrobenzene-d5 80.8 14.0-149
(S) 2-Fluorobiphenyl 79.4 34.0-125
Laboratory Control Sample (LCS)
(LCS) R3876461-1 12/28/22 12:35
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Anthracene 0.0800 0.0682 85.3 50.0-126
Acenaphthene 0.0800 0.0687 85.9 50.0-120
Acenaphthylene 0.0800 0.0683 85.4 50.0-120
Benzo(a)anthracene 0.0800 0.0732 91.5 45.0-120
Benzo(a)pyrene 0.0800 0.0609 76.1 42.0-120
Benzo(b)fluoranthene 0.0800 0.0683 85.4 42.0-121
Benzo(g,h,i)perylene 0.0800 0.0666 83.3 45.0-125
Benzo(k)fluoranthene 0.0800 0.0686 85.8 49.0-125
Chrysene 0.0800 0.0736 92.0 49.0-122
Dibenz(a,h)anthracene 0.0800 0.0690 86.3 47.0-125
Fluoranthene 0.0800 0.0717 89.6 49.0-129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1980069
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1570312-01,02,03,04,05,06
Laboratory Control Sample (LCS)
(LCS) R3876461-1 12/28/22 12:35
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Fluorene 0.0800 0.0704 88.0 49.0-120
Indeno(1,2,3-cd)pyrene 0.0800 0.0718 89.8 46.0-125
Naphthalene 0.0800 0.0671 83.9 50.0-120
Phenanthrene 0.0800 0.0704 88.0 47.0-120
Pyrene 0.0800 0.0737 92.1 43.0-123
1-Methylnaphthalene 0.0800 0.0671 83.9 51.0-121
2-Methylnaphthalene 0.0800 0.0692 86.5 50.0-120
2-Chloronaphthalene 0.0800 0.0669 83.6 50.0-120
(S) p-Terphenyl-d14 89.8 23.0-120
(S) Nitrobenzene-d5 87.3 14.0-149
(S) 2-Fluorobiphenyl 83.2 34.0-125
L1570312-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1570312-02 12/28/22 16:43 • (MS) R3876461-3 12/28/22 17:00 • (MSD) R3876461-4 12/28/22 17:18
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Anthracene 0.0780 0.163 0.122 0.127 0.000 0.000 1 10.0-145 J6 J6 4.02 30
Acenaphthene 0.0780 1.59 1.41 1.02 0.000 0.000 1 14.0-127 V J3 V 32.1 27
Acenaphthylene 0.0780 ND 0.336 0.296 431 387 1 21.0-124 J5 J5 12.7 25
Benzo(a)anthracene 0.0780 1.50 0.130 0.319 0.000 0.000 1 10.0-139 V J3 V 84.2 30
Benzo(a)pyrene 0.0780 1.26 0.0868 0.278 0.000 0.000 1 10.0-141 V J3 V 105 31
Benzo(b)fluoranthene 0.0780 1.52 0.0927 0.314 0.000 0.000 1 10.0-140 V J3 V 109 36
Benzo(g,h,i)perylene 0.0780 0.752 0.0777 0.185 0.000 0.000 1 10.0-140 V J3 V 81.7 33
Benzo(k)fluoranthene 0.0780 0.556 0.0658 0.154 0.000 0.000 1 10.0-137 V J3 V 80.3 31
Chrysene 0.0780 1.17 0.110 0.299 0.000 0.000 1 10.0-145 V J3 V 92.4 30
Dibenz(a,h)anthracene 0.0780 0.191 0.0590 0.0898 0.000 0.000 1 10.0-132 J6 J3 J6 41.4 31
Fluoranthene 0.0780 1.29 0.300 0.334 0.000 0.000 1 10.0-153 V V 10.7 33
Fluorene 0.0780 2.01 1.77 1.18 0.000 0.000 1 11.0-130 V J3 V 40.0 29
Indeno(1,2,3-cd)pyrene 0.0780 0.919 0.0797 0.223 0.000 0.000 1 10.0-137 V J3 V 94.7 32
Naphthalene 0.0780 6.30 4.88 5.25 0.000 0.000 1 10.0-135 E V E V 7.31 27
Phenanthrene 0.0780 2.74 2.84 2.13 128 0.000 1 10.0-144 V 28.6 31
Pyrene 0.0780 1.14 0.336 0.357 0.000 0.000 1 10.0-148 V V 6.06 35
1-Methylnaphthalene 0.0780 13.2 9.43 12.0 0.000 0.000 1 10.0-142 E V E V 24.0 28
2-Methylnaphthalene 0.0780 23.5 17.2 20.3 0.000 0.000 1 10.0-137 E V E V 16.5 28
2-Chloronaphthalene 0.0780 ND 0.0524 0.0494 67.2 64.7 1 29.0-120 5.89 24
(S) p-Terphenyl-d14 81.1 86.8 23.0-120
(S) Nitrobenzene-d5 167 291 14.0-149 J1 J1
(S) 2-Fluorobiphenyl 95.4 78.8 34.0-125
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1980069
Semi Volatile Organic Compounds (GC/MS) by Method 8270C-SIM L1570312-01,02,03,04,05,06
L1570312-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1570312-02 12/28/22 16:43 • (MS) R3876461-3 12/28/22 17:00 • (MSD) R3876461-4 12/28/22 17:18
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Sample Narrative:
OS: Surrogate failure due to matrix interference
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
E The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial
calibration (ICAL).
J The identification of the analyte is acceptable; the reported value is an estimate.
J1 Surrogate recovery limits have been exceeded; values are outside upper control limits.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
J7 Surrogate recovery cannot be used for control limit evaluation due to dilution.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS
¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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APPENDIX D
PROFESSIONAL QUALIFICATIONS
Eric Routh
Project Scientist
21 B Street
Burlington, MA 01803
Mobile: 240.338.0731
SUMMARY OF EXPERIENCE
Mr. Routh is a project scientist specializing in Phase I and Phase II Environmental Site Assessments in the
commercial real estate industry. Mr. Routh has conducted numerous pre-acquisition/due diligence
environmental assessments for a wide range of properties throughout the Mid-Atlantic region. These
assessments have been performed to evaluate site conditions, potential off-site liabilities, historic site
and vicinity usage, environmental control systems, and site remediation costs in order to advise
prospective buyers, lenders, current operators, and owners of potential and existing environmental
concerns. Sites inspected include multi-family residential, commercial, retail, and industrial properties.
RELEVANT PROJECT EXPERIENCE
Phase I Environmental Site Assessments: Mr. Routh has conducted ASTM Phase I Environmental
Site Assessments for a variety of properties located within the Mid-Atlantic region. These properties
have included commercial, retail, industrial, and multi-family residential properties. ASTM investigations
include correspondence and consultation with Federal, state, and local government offices.
Phase II Subsurface Investigation: Mr. Routh has completed numerous Phase II subsurface
investigation projects, with field and project management experience associated with soil and
groundwater monitoring. Mr. Routh has prepared schedules, work plans, health and safety plans, and
resulting Phase II reports.
EDUCATION
M.S. Environmental Sciences and Policy, Johns Hopkins University, Baltimore, MD 2013
B.S. Natural Resource Sciences, University of Maryland, College Park, MD 2008
PROFESSIONAL TRAINING/REGISTRATIONS
OSHA 29 CFR 1910.120 40-Hour Hazardous Waste Operations & Emergency Response Training,
2014
Maryland Department of the Environment Erosion and Sediment Control Responsible Personnel
Certification (Green Card)
ASTM E 1527 Phase I Environmental Site Assessment (ESA) Training
AHERA 24-hour Asbestos Inspector Accreditation
U.S. Department of Housing and Urban Development (HUD) Lead Based Paint Visual Assessment
Training Course
Stephanie Clorety
Project Manager Site Investigation and
Remediation Group
21 B Street
Burlington, MA 01803
Office: 443.695.6135
Bruce Speidel
Senior Program Director
2035 Ober Brienz Lane
Franklin, TN 37064
707.8291
SUMMARY OF EXPERIENCE
Stephanie Clorety, Project Manager Site Investigation and Remediation Group has extensive
experience in environmental geology since 1999. Mrs. Clorety has completed site investigations and
remedial actions including Phase I Environmental Site Assessments, Phase II subsurface investigations, Site
Characterizations, UST removals, and landfill compliance sampling and monitoring, sewer outfall sampling,
health and safety construction/demolition monitoring, remediation system observation and maintenance,
drinking water sampling, and radon surveys.
Mrs. Clorety has conducted multiple site assessments and regulatory site closures for a wide range of
properties throughout the United States, Canada and Aruba. These assessments have been performed to
evaluate site conditions, potential off-site liabilities, environmental control systems, and site remediation
costs in order to advise prospective buyers, current operators, and owners of potential and existing
environmental concerns.
RELEVANT PROJECT EXPERIENCE
Conducted ASTM Phase I Environmental Site Assessments, Environmental Site Screenings, soil,
groundwater, and leachate sampling, landfill gas monitoring and construction oversight for landfill caps.
Conducted the landfill closure oversight including liner and cap installation, installation of landfill venting
systems, installation and sampling of groundwater and vapor monitoring system. Completed the
annual/semi-annual/quarterly compliance sampling including groundwater, vapor, leachate and drinking
water sampling and regulatory reporting for landfills located in Massachsetts, Connecticut, Pennsylvania
and Maryland.
Completed subsurface investigation at property types ranging from commercial to residential. Task
manager for multiple gasoline refineries and terminals for conducting or general oversight of the weekly,
monthly, and quarterly gauging, bailing, sampling and observation and maintenance of remediation systems.
In charge of the sewer outfall sampling for one of the petroleum refineries. I also completed subsurface
investigation at various gasoline service stations across Maryland, Pennsylvania and Virginia. Task manager
for multiple gasoline service stations for conducting or general oversight of the weekly, monthly, and
quarterly gauging, bailing, sampling and observation and maintenance of remediation systems. Completed
oversight of the UST removals at several gasoline service stations across Maryland Pennsylvania and
Virginia.
Completed subsurface investigation at property types such as industrial, commercial, landfills, refineries
and residential. The subsurface investigations included direct-push sampling, hollow stem auger and mud
rotary drilling for the installation of monitoring wells and soil vapor points. Completed subsurface
investigations and oversight of the UST removals at various properties across Maryland, Virginia,
Pennsylvania, and West Virginia. Assisted in processing several commercial and former industrial
properties through state’s Voluntary Clean Up/Brownfield Programs and Pennsylvania’s Act 2 Program.
Completed construction oversight air monitoring and was the site health and safety officer during the
monitoring events.
EDUCATION
Bachelor of Science, Environmental Geology - Ohio University
Stephanie Clorety
Project Manager Site Investigation and
Remediation Group
21 B Street
Burlington, MA 01803
Office: 443.695.6135
Bruce Speidel
Senior Program Director
2035 Ober Brienz Lane
Franklin, TN 37064
707.8291
PROFESSIONAL REGISTRATIONS
40-Hour OSHA Hazardous Worker/ 8 Hour Refresher
Maryland Certified Asbestos Inspector
Maryland Certified Lead Inspector
Professional Geologist Tennessee
Professional Geologist Louisanna
Lisenced Remediation Specialist West Virginia
Bruce Speidel, P.G.
Senior Program Director
21 B Street
Burlington, MA 01803
Office: 410.552.1405 Mobile: 410.707.8291
SUMMARY OF EXPERIENCE
Mr. Speidel has over 30 years experience in the environmental and engineering consulting fields. Mr. Speidel
has performed and/or managed site investigations and remedial actions at over 5,000 sites, including Phase
I Environmental Site Assessments, Phase II subsurface investigations, Site Characterizations, UST removals,
and construction materials inspections/testing at various industrial, commercial, and residential development
sites throughout the United States, Canada, Mexico, and Puerto Rico. He has also conducted asbestos
surveys and third-party desk reviews. In addition, he has been involved with numerous regulatory closure
projects as well as a large remediation projects at commercial and industrial sites. He is a Registered
Professional Geologist in Arizona, Delaware, Louisiana, Pennsylvania, Tennessee, Texas, Virginia, and
Washington.
Mr. Speidel has worked with corporate environmental officers, numerous Wall Street lending institutions,
legal counsel, investment companies, and real estate brokers to develop strategies for managing properties
with environmental concerns. Mr. Speidel currently oversees the day to day operations and leadership of
EBI’s Subsurface Investigation and Remediation (SIR) group in the Mid-Atlantic, Southeast, Central, and
West regions. Mr. Speidel is currently responsible for managing environmental due diligence investigation
for property acquisition and financing, including underground storage tank removals, state voluntary
cleanup programs, environmental site assessments, subsurface site investigations, site characterizations,
third party document reviews including regulatory case history reviews, and cost estimating associated
with property transactions and evaluations; and other due diligence related activities; providing senior
level managerial, technical, and operational project coordination, and client relations.
RELEVANT PROJECT EXPERIENCE
Conducted and managed over 3,500 Phase I Environmental Site Assessments for sites throughout the
United States, Canada, Mexico, and Puerto Rico in accordance with ASTM E 1527.
Designed and conducted/managed over 2,000 Phase II Environmental Site Assessments throughout
the United States.
Developed in-house Guidance Manual for conducting Phase II Environmental Site Assessments.
Actively participated in the investigative phase and construction management of a $5 million
remediation project at a stainless steel mill. Responsibilities included site supervision of the
subcontractors performing the remedial activities. Remedial activities included site grading and
development, sediment and erosion control, and the installation of a vertical barrier wall and
associated hydraulic control system that was designed to remediate groundwater contaminated with
petroleum hydrocarbons, heavy metals, and acids.
Operated and maintained groundwater remediation systems.
Conducted groundwater monitoring programs.
Provided geologist services for environmental and geotechnical subsurface investigations.
Extensive experience in construction materials testing and inspections for commercial buildings,
schools, nuclear power plants, residential developments, stormwater management ponds, and
roadway construction.
Bruce Speidel, P.G.
Senior Program Director
21 B Street
Burlington, MA 01803
Office: 410.552.1405 Mobile: 410.707.8291
EDUCATION
Bachelor of Science in Geology (1987), West Virginia University, Morgantown, West Virginia
University of Maryland, College Park, MD (1994). Completed course in Hydrogeology
CONTINUING EDUCATION
Phase II Environmental Site Assessment Process (1999); ASTM Technical & Professional Training Course
Environmental Forensics: Methods and Application (2004); National Groundwater Association
Environmental Education Course
Practical Rock Slope Engineering, Part I; AEG/BWH (2004)
Understanding Migration, Assessment, and Remediation of Non-Aqueous Phase Liquids (LNAPLS and DNAPLS)
(November 2005); National Groundwater Association Environmental Education Course
National Groundwater Association Focus Conference on Eastern Regional Groundwater Issues (September
2006)
Science and Myths of Indoor Inhalation Pathway (2007); National Groundwater Association
Environmental Education Course
Assessment of Vapor Intrusion into Structures on Property Involved in Real Estate Transactions (2008); ASTM
Technical & Professional Training Course
Environmental Isotopes in Groundwater Resources and Contaminant Hydrogeology (2008); National
Groundwater Association Environmental Education Course
Site Remediation Basics (New Jersey Department of Environmental Protection); Rutgers University - New
Jersey Agricultural Experiment Station, Office of Continuing Professional Education (2009)
Site Remediation Reform Act and LSRP Program; Rutgers University - New Jersey Agricultural Experiment
Station, Office of Continuing Professional Education (2009)
Fundamentals of Groundwater Geochemistry; National Groundwater Association Environmental
Education Course (2010)
Estimating Times of Remediation Associated with MNA and Contaminant Source Removal; National
Groundwater Association Environmental Education Course (2011)
Light Nonaqueous-Phase Liquids (LNAPLs): Science, Management, and Technology course (2012);
Interstate Technology Regulatory Council; (ITRC)
Effective Technical Writing: Principals and Strategies; National Groundwater Association Environmental
Education Course (2013)
Hydrogeology Fundamentals and Refresher; National Groundwater Association Environmental Education
Course (2013)
Groundwater Sampling and Environmental Monitoring, National Groundwater Association Environmental
Education Course (2013)
Introduction to Mountain Hydrogeology; National Groundwater Association Environmental Education
Course (2014)
The Vapor Intrusion Risk Pathway: A Practical Guide; Hartman Environmental Geoscience Training (2014)
Environmental Forensics; National Groundwater Association Environmental Education Course (2016)
The Vapor Intrusion Risk Pathway: A Practical Guide; Hartman Environmental Geoscience Training (2018)
Vapor Intrusion, Remediation, and Site Closure; Air & Waste Management (2018)
Bruce Speidel, P.G.
Senior Program Director
21 B Street
Burlington, MA 01803
Office: 410.552.1405 Mobile: 410.707.8291
PROFESSIONAL REGISTRATIONS
Professional Geologist, Arizona #49415
Professional Geologist, Delaware #S4-0001101
Professional Geologist, Louisiana #113
Professional Geologist, Pennsylvania #004004
Professional Geologist, South Carolina #2769
Professional Geologist, Tennessee #TN4390
Professional Geologist, Texas #10532
Professional Geologist, Virginia #2801 001579
Professional Geologist, Washington #3007
Asbestos Building Inspector
Asbestos Management Planner
OSHA 29 CFR 1910.120 40 Hour HAZWOPER
APPENDIX E
GPR REPORT
501 Cambria Avenue, Suite 281, Bensalem, PA 19020
215-366-7389
eastcoastgeophysics.com
Date:
12/21/23
Site Location:
1514 Main Street
Ramseur, North Carolina
Attention:
EBI Consulting
21 B Street, Burlington, Massachusetts, 01803
Regards:
Brian Halvorsen
East Coast Geophysics Inc.
501 Cambria Avenue Suite 281, Bensalem, Pennsylvania, 19020
East Coast Geophysics Inc 501 Cambria Avenue Suite 281, Bensalem, PA 19020 215-366-7389
1
1. BACKGROUND AND PROJECT OBJECTIVES
The subject property at 1514 Main Street in Ramseur, North Carolina consists of an active US
Post office. Surface conditions consistent of concrete, asphalt, soil, and grass. Site project
objectives are:
• Locate all detectable underground utilities adjacent to the client proposed soil borings.
• Scan the subject property and client specified areas for underground anomalous features
such as underground storage tanks (UST), UST piping, and former excavations.
2. EQUIPMENT
This project used the following equipment to perform the geophysical survey on the property.
• GSSI SIR-3000 Cart Mounted Ground Penetrating Radar System
Ground Penetrating Radar is a non-invasive geophysical method in which electromagnetic
pulses probe the subsurface, allowing targets to be imaged in real time. The EM pulses that
are transmitted into the subsurface are reflected from various interfaces within the ground,
including soil horizons, ground water, and manmade features such as underground storage
tanks and utilities. The GPR antenna consists of a transmitter, which is used to create the EM
pulse, and a receiver which collects returning signals. The high frequency waves created by
the antenna can be generated in a range of 10 MHz to 2.6 GHz. The frequency of the antenna
will vary the depth of penetrations, signal clarity, and attenuation into the subsurface. The
antenna used for general field work by ECG is 400 MHz; this frequency range has the
capability to transmit to a depth of up to 10 feet below ground surface. Surface and
subsurface conditions can greatly reduce the effective depth of the signal penetration; these
conditions include conductive soils, slag/fill material and standing water.
• Radiodetection RD7000+
RD7000 is an advanced high-range precision utility detector capable of detecting utilities up
to 15 feet below ground surface. The RD7000+ has the capability of locating a variety of
pipes and cables using either passive or active modes. Passive signals can be traced with only
the transmitter using “natural” signals present in many conductors. These signals can be
generated from an array of sources including power cables, power system return currents, and
long wave radio frequencies. Active signals are known AC frequencies induced onto a target
pipe or cable. User induced signals can help positively identify lines throughout areas of
congested utilities.
• Fisher TW-6 Pipe and Cable Locator
The Fisher TW-6 Pipe and cable locator uses electromagnetic induction to locate conductive
materials, such as manholes, tanks, pipes, cables, and other metallic materials in the
subsurface. The transmitter generates an AC current which produces an electromagnetic field
similar to a dipole magnet. When the transmitter passes over a conductive feature, the
generated electromagnetic field becomes distorted as a result of the interference with the
natural electromagnetic field created by the conductive feature. The distortion of the
generated field is detected by the receiver which emits a tone that is correlated to the
conductivity of the feature.
East Coast Geophysics Inc 501 Cambria Avenue Suite 281, Bensalem, PA 19020 215-366-7389
2
3. PROCEDURE
ECG personnel began with a utility survey utilizing active detection with the RD-7000+. This is
done by directing hooking up to known surface features across the site such as valves, exposed
lifts, and fill ports. The surveyor then performed a passive scan with the RD-7000+ receiver to
detect any energized utilities that may have not been located with the active scan. Any detected
utilities were then marked in the field.
ECG personnel then walked across the survey area with the TW-6 in 3-5 foot spacing increments.
The approximate size and shape of any conductive targets detected was then marked in white and
will be further investigated with GPR.
GPR was then utilized to confirm the approximate depth of any utilities detected with the RD-
7000+ and the size, shape, and depth of any anomalies located with the TW-6. ECG personnel
then scanned the remaining portions of the property in 3-5 foot spacing increments for any other
anomalous features or utilities not detected with the RD-7000+ or TW-6.
4. RESULTS
• Underground Utilities – No utilities were detected in proximity to the sample locations,
• Potential Former Excavation
o A potential former excavation was detected with GPR transects. The feature is
located on the northwest corner of the subject building. The potential former
excavation measures approximately 13 feet by 6 feet. GPR transects imaged
disturbed soils above the anomalous area. The feature is located below a cutout
concrete pad and an AST.
No other anomalous features were observed at the subject site.
5. SITE LIMITATIONS
• Ground Penetrating Radar – GPR depth of penetration was limited to 1-3 feet bgs. The
limiting factor was signal attenuation from near surface soils
• Metallic Structures – The TW-6 cannot be utilized within close proximity to metallic
features such as, transformers, vehicles, and reinforced concrete.
6. DISCLAIMER
The limitations of a geophysical survey from both the site and equipment are important to
consider when performing intrusive work at a survey site. The equipment is unable to maintain a
constant depth of penetration or a constant level of effectiveness over the course of a survey due
to subsurface and environmental conditions. The results provided both in this report and in the
field should be used in conjunction with other methods including but not limited to, site plans, as-
builts, sanborn maps, field observations, public-mark out services, soft-digging, pre-clearing, and
historical documentation of the site. No survey or survey method can accurately show an exact
image of all subsurface conditions. The presence of non-detectable subsurface utilities and
structures is always a risk at any site. Please take caution when proceeding with invasive work.
A/C UNITPOTENTIALFORMEREXCAVATIONASTSUBJECTBUILDINGOFF-SITEBUILDINGOFF-SITEBUILDINGMAIN STREETSITECLIENTPROJECT NO.DRAWING NO.SHEET NO.SCALEDATEDRAWN 1514 MAIN STREET RAMSEUR, NORTH CAROLINAEBI1221221221231/3/23BRH1 OF 11 : 20NOTES:East Coast Geophysics, Inc. shall not beliable for damages of any kind arising out ofthe use of this information. Drawings aregeoreferenced based on satellite imageryand are not considered to be survey quality.These drawings are intended to be used asreference only.LEGENDELECTRICEEE02040105STORM DRAINSDSDSDSTORM DRAINSANITARY SEWERGASGGGWATERWWWSSSSSS